SAS Output

BQS Organic Blind Sample Project

False Positive and Negative Report for

Schedule: 2060

Analyte	TestIDCode	CASNumber	# Samples Spiked	# False Negatives	# Samples Not Spiked	# False Positives
2,4-D	39732LCM29	94-75-7	92	1	104	0
2,4-D + 2,4-D METHYL ESTER (SUM)	66496CAL13	000-08-01	67	1	88	7
2,4-D METHYL ESTER	50470LCM29	1928-38-7	78	1	118	2
2,4-DB	38746LCM29	94-82-6	84	0	112	4
2-HYDROXYATRAZINE (2-HYDROXY-4-ISOPROPYLAMINO-6-ETHYLAMINO-S-TRIAZINE) OIET	50355LCM29	2163-68-0	44	0	130	36
3(4-CHLOROPHENYL) METHYL UREA	61692LCM29	5352-88-5	92	0	104	0
3-HYDROXYCARBOFURAN	49308LCM29	16655-82-6	85	0	111	1
ACIFLUORFEN	49315LCM29	50594-66-6	86	1	110	0
ALDICARB	49312LCM29	116-06-3	85	1	111	0
ALDICARB SULFONE	49313LCM29	1646-88-4	83	0	113	9
ALDICARB SULFOXIDE	49314LCM29	1646-87-3	86	0	77	3
ATRAZINE	39632LCM29	1912-24-9	85	0	111	1
BENDIOCARB	50299LCM29	22781-23-3	87	1	109	4
BENOMYL	50300LCM29	17804-35-2	85	0	111	0
BENSULFURON-METHYL	61693LCM29	83055-99-6	54	0	120	0
BENTAZON	38711LCM29	25057-89-0	85	2	111	2
BROMACIL	04029LCM29	314-40-9	85	0	111	0
BROMOXYNIL	49311LCM29	1689-84-5	85	0	111	1
CAFFEINE	50305LCM29	58-08-2	82	0	114	1
CARBARYL	49310LCM29	63-25-2	84	0	112	0
CARBOFURAN	49309LCM29	1563-66-2	84	0	112	0
CHLORAMBEN, METHYL ESTER	61188LCM29	7286-84-2	84	23	112	3
CHLORIMURON ETHYL	50306LCM29	90982-32-4	62	0	112	0
CLOPYRALID	49305LCM29	1702-17-6	85	5	111	0
CYCLOATE	04031LCM29	1134-23-2	84	0	112	1
DACTHAL MONOACID	49304LCM29	887-54-7	69	6	127	0
DEETHYLATRAZINE (DESETHYL ATRAZINE) (2-CHLORO-4-ISOPROPYLAMINO-6-S-TRIAZINE) CIAT	04040LCM29	6190-65-4	87	0	109	0
DEISOPROPYLATRAZINE (2-CHLORO-6-ETHYLAMINO-4-AMINO-S-TRIAZINE) CEAT	04038LCM29	1007-28-9	88	1	108	0
DICAMBA	38442LCM29	1918-00-9	87	12	109	0
DICHLOROPROP (DICHLORPROP)	49302LCM29	120-36-5	86	0	110	0
DINOSEB	49301LCM29	88-85-7	87	0	109	1
DIPHENAMID	04033LCM29	957-51-7	84	0	112	0
DIURON	49300LCM29	330-54-1	84	0	112	0
FENURON	49297LCM29	101-42-8	86	0	110	0
FLUMETSULAM	61694LCM29	98967-40-9	85	2	111	0
FLUOMETURON	38811LCM29	2164-17-2	84	1	112	0
IMAZAQUIN	50356LCM29	81335-37-7	84	0	112	0
IMAZETHAPYR	50407LCM29	81335-77-5	85	0	111	0
IMIDACLOPRID	61695LCM29	138261-41-3	82	2	114	0
LINURON	38478LCM29	330-55-2	84	0	112	0
MCPA	38482LCM29	94-74-6	87	0	109	0
MCPB	38487LCM29	94-81-5	85	9	111	0
METALAXYL	50359LCM29	57837-19-1	86	0	110	0
METHIOCARB	38501LCM29	2032-65-7	86	1	110	0
METHOMYL	49296LCM29	16752-77-5	85	0	111	0
METSULFURON METHYL	61697LCM29	74223-64-6	85	1	111	0
NEBURON	49294LCM29	555-37-3	84	0	112	0
NICOSULFURON	50364LCM29	111991-09-4	80	13	116	0
NORFLURAZON	49293LCM29	27314-13-2	84	0	112	0
ORYZALIN	49292LCM29	19044-88-3	86	1	110	0
OXAMYL	38866LCM29	23135-22-0	85	0	111	1
PICLORAM	49291LCM29	1918-02-1	84	9	112	2
PROPHAM	49236LCM29	122-42-9	86	1	110	0
PROPICONAZOLE (TILT)	50471LCM29	60207-90-1	84	0	112	0
PROPOXUR	38538LCM29	114-26-1	83	0	113	0
SIDURON	38548LCM29	1982-49-6	84	0	112	0
SULFOMETURON METHYL	50337LCM29	74222-97-2	71	0	103	0
TEBUTHIURON	82670LCM29	34014-18-1	80	0	116	0
TERBACIL	04032LCM29	5902-51-2	87	0	109	1
TRICLOPYR	49235LCM29	55335-06-3	85	0	111	0

BQS Organic Blind Sample Program

False Positives & False Negatives

2,4-D

Schedule: 2060 Testid: 39732LCM29

Link to Individual Chart

False Positive & Negative Listing for 2,4-D

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20073380128	Abs 071607LC: 50 µl	0.02	01/03/08	< 0.02	0.2015

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

2,4-D + 2,4-D METHYL ESTER (SUM)

Schedule: 2060 Testid: 66496CAL13

Link to Individual Chart

False Positive & Negative Listing for 2,4-D + 2,4-D METHYL ESTER (SUM)

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20073380128	Abs 071607LC: 50 µl	0.02	01/03/08	< 0	0.5205
False Positive	20121670022	Supelco LB92941: 20 µl	0.06	07/09/12	E 0.46	0
	20121810017	Spex Organics T1120525009: 50 µl & Supelco LB92941: 50 µl	0.06	07/18/12	E 1.11	0
	20122020005	NSI 062612-01: 20 µl & NSI 718L-01-01: 20 µl & ChemService 396400: 20 µl	0.06	08/07/12	E 0.675	0
	20122300023	Spex Organics T1120525009: 20 µl & NSI 062612-01: 20 µl & NSI 718L-01-01: 20 µl	0.06	09/13/12	E 0.407	0
	20122570123	NSI 062612-01: 20 µl & NSI 718L-01-01: 20 µl & Restek A088383: 20 µl	0.06	09/28/12	E 0.687	0
	20123140094	Abs 052312: 20 µl & NSI 062612-01: 20 µl & NSI 718L-01-01: 20 µl	0.06	12/05/12	E 0.37	0
	20123260035	Supelco LB92941: 20 µl & ChemService 396400: 20 µl	0.06	12/05/12	E 0.361	0

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

2,4-D METHYL ESTER

Schedule: 2060 Testid: 50470LCM29

Link to Individual Chart

False Positive & Negative Listing for 2,4-D METHYL ESTER

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20073380128	Abs 071607LC: 50 µl	0.04	01/03/08	< 0.2	0.319
False Positive	20101720152	NSI 090309-01HPLC: 80 µl	0.2	07/01/10	E 0.04	0
	20101830111	NWQL LCL11SP079A: 50 µl & NWQL LCL11SP079B: 50 µl	0.2	07/27/10	E 0.005	0

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

2,4-DB

Schedule: 2060 Testid: 38746LCM29

Link to Individual Chart

False Positive & Negative Listing for 2,4-DB

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
False Positive	20070860102	Ultra CC-2418: 75 µl	0.02	04/10/07	E 0.001
	20071860003	Ultra CC-2418: 75 µl	0.02	07/25/07	E 0.001
	20092260010	Restek A063332: 50 µl & Restek A062398: 50 µl	0.02	09/02/09	E 0.009
	20102160005	Spex Organics T1090828008: 80 µl	0.02	09/01/10	E 0.006

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

2-HYDROXYATRAZINE (2-HYDROXY-4-ISOPROPYLAMINO-6-ETHYLAMINO-S-TRIAZINE) OIET

Schedule: 2060 Testid: 50355LCM29

Link to Individual Chart

False Positive & Negative Listing for 2-HYDROXYATRAZINE (2-HYDROXY-4-ISOPROPYLAMINO-6-ETHYLAMINO-S-TRIAZINE) OIET

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
False Positive	20070720033	Accu B6070187: 75 µl	0.08	03/28/07	E 0.009
	20070800016	ChemService 363-120B: 50 µl	0.08	04/10/07	E 0.008
	20071500018	Accu B6070187: 50 µl	0.08	06/18/07	E 0.004
	20072200099	Accu B6070187: 75 µl	0.08	08/25/07	E 0.007
	20080800003	Protocol I1070803003: 50 µl	0.04	04/04/08	E 0.006
	20081150079	Protocol I1070803003: 50 µl	0.04	05/16/08	E 0.002
	20081840007	Restek A053251: 50 µl	0.04	07/23/08	E 0.011
	20082130006	Protocol I1070803003: 50 µl	0.04	08/14/08	E 0.015
	20082260236	Restek A053251: 50 µl	0.04	08/28/08	E 0.037
	20091320004	ERA 0813-08-07Polar: 30 µl	0.06	05/28/09	E 0.011
	20092040200	ERA 0813-08-07Polar: 30 µl	0.06	08/06/09	E 0.014
	20092460256	ERA 0813-08-07Polar: 50 µl	0.06	09/22/09	E 0.018
	20101340151	Accu 209081166: 80 µl	0.06	06/10/10	E 0.006
	20101650030	ChemService 430-40B: 40 µl	0.06	06/30/10	E 0.004
	20102180094	ChemService 430-40B: 80 µl	0.06	08/31/10	E 0.009
	20102530004	ChemService 430-40B: 80 µl	0.06	10/27/10	. 0.078
	20103510059	Restek A075600: 40 µl	0.06	01/04/11	. 0.036
	20110340008	Crescent 163162: 40 µl	0.06	02/25/11	. 0.03
	20110490034	ChemService 448-45B: 40 µl	0.06	03/07/11	. 0.059
	20110620084	Restek A075600: 40 µl	0.06	03/23/11	. 0.024
	20110910082	Crescent 163162: 100 µl	0.06	04/14/11	. 0.036
	20111190183	Restek A075600: 100 µl	0.06	05/20/11	. 0.033
	20111330149	Crescent 163162: 40 µl	0.06	05/21/11	. 0.02
	20111540006	Restek A075600: 40 µl	0.06	06/11/11	. 0.024
	20111750004	Crescent 163162: 40 µl	0.06	07/20/11	. 0.011
	20111960035	Crescent 163162: 100 µl	0.06	07/19/11	. 0.019
	20112170175	Restek A075600: 40 µl	0.06	09/06/11	. 0.012
	20112450024	Restek A075600: 100 µl	0.06	09/14/11	. 0.042
	20113130087	Restek A075600: 40 µl	0.06	11/29/11	. 0.013
	20113500019	Crescent 163162: 100 µl	0.06	01/05/12	. 0.008
	20120260062	Restek A075600: 100 µl	0.06	02/14/12	. 0.02
	20120470081	Crescent 163162: 40 µl	0.06	03/07/12	. 0.018
	20120760112	Restek A075600: 40 µl	0.06	03/27/12	. 0.016
	20120960123	Restek A075600: 40 µl	0.06	05/03/12	. 0.016
	20121310031	Restek A075600: 100 µl	0.06	05/22/12	. 0.021
	20121460002	Crescent 163162: 40 µl	0.06	06/21/12	. 0.014

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

3-HYDROXYCARBOFURAN

Schedule: 2060 Testid: 49308LCM29

Link to Individual Chart

False Positive & Negative Listing for 3-HYDROXYCARBOFURAN

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Positive	20092960006	Crescent 08LL073: 40 µl	0.04	11/19/09	E 0.003	0

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

ACIFLUORFEN

Schedule: 2060 Testid: 49315LCM29

Link to Individual Chart

False Positive & Negative Listing for ACIFLUORFEN

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20103020153	Crescent 163162: 40 µl	0.04	11/30/10	< 0.04	0.0633663

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

ALDICARB

Schedule: 2060 Testid: 49312LCM29

Link to Individual Chart

False Positive & Negative Listing for ALDICARB

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20080290026	Crescent 07GG007: 50 µl	0.12	02/12/08	< 0.12	0.1480952

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

ALDICARB SULFONE

Schedule: 2060 Testid: 49313LCM29

Link to Individual Chart

False Positive & Negative Listing for ALDICARB SULFONE

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
False Positive	20070240002	Ultra CC-2418: 50 µl	0.08	02/09/07	E 0.006
	20070640064	Ultra CC-2418: 50 µl	0.08	03/28/07	E 0.005
	20071150010	Supelco LB40676: 75 µl	0.08	05/11/07	E 0.007
	20071220023	Supelco LB40676: 20 µl	0.08	05/11/07	E 0.002
	20071360138	Ultra CC-2418: 75 µl	0.08	06/02/07	E 0.008
	20071640021	Supelco LB40676: 75 µl	0.08	06/25/07	E 0.006
	20071860003	Ultra CC-2418: 75 µl	0.08	07/25/07	E 0.008
	20092960006	Crescent 08LL073: 40 µl	0.08	11/19/09	E 0.003
	20093380008	NSI 090309-01HPLC: 80 µl	0.08	12/29/09	E 0.006

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

ALDICARB SULFOXIDE

Schedule: 2060 Testid: 49314LCM29

Link to Individual Chart

False Positive & Negative Listing for ALDICARB SULFOXIDE

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
False Positive	20122210007	Abs 052312: 20 µl & Restek A088383: 20 µl	0.08	08/22/12	E 0.034
	20123040156	Abs 052312: 50 µl & ChemService 396400: 50 µl	0.08	11/13/12	E 0.046
	20123490150	Spex Organics T1120525009: 50 µl & Restek A088383: 50 µl	0.08	12/21/12	E 0.031

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

ATRAZINE

Schedule: 2060 Testid: 39632LCM29

Link to Individual Chart

False Positive & Negative Listing for ATRAZINE

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Positive	20100630038	Crescent 08LL073: 40 µl	0.04	03/17/10	E 0.0008	0

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

BENDIOCARB

Schedule: 2060 Testid: 50299LCM29

Link to Individual Chart

False Positive & Negative Listing for BENDIOCARB

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20080860017	Crescent 07GG007: 50 µl	0.04	04/04/08	< 0.04	0.070373
False Positive	20070720033	Accu B6070187: 75 µl	0.04	03/28/07	E 0.037	0
	20072200099	Accu B6070187: 75 µl	0.04	08/25/07	E 0.005	0
	20083110007	NSI 081208-01Polar: 50 µl	0.04	11/19/08	E 0.006	0
	20091550186	NSI 081208-01Polar: 30 µl	0.04	06/17/09	E 0.002	0

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

BENTAZON

Schedule: 2060 Testid: 38711LCM29

Link to Individual Chart

False Positive & Negative Listing for BENTAZON

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20071290015	Restek A046748: 75 µl	0.02	06/02/07	< 0.02	0.0671709
	20101480008	Crescent 08LL073: 40 µl	0.06	06/17/10	< 0.06	0.0705175
False Positive	20071150010	Supelco LB40676: 75 µl	0.02	05/11/07	E 0.001	0
	20073060022	Ultra CD-2088: 50 µl	0.04	11/28/07	E 0.002	0

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

BROMOXYNIL

Schedule: 2060 Testid: 49311LCM29

Link to Individual Chart

False Positive & Negative Listing for BROMOXYNIL

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Positive	20070580108	Protocol F1060804006: 20 µl	0.12	03/12/07	E 0.0007	0

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

CAFFEINE

Schedule: 2060 Testid: 50305LCM29

Link to Individual Chart

False Positive & Negative Listing for CAFFEINE

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Positive	20092960006	Crescent 08LL073: 40 µl	0.08	11/19/09	. 0.252	0

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

CHLORAMBEN, METHYL ESTER

Schedule: 2060 Testid: 61188LCM29

Link to Individual Chart

False Positive & Negative Listing for CHLORAMBEN, METHYL ESTER

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20073380128	Abs 071607LC: 50 µl	0.1	01/03/08	< 0.1	0.341
	20080150157	Accu B7070230: 50 µl	0.1	02/12/08	< 0.1	0.3474628
	20080740019	Accu B7070230: 50 µl	0.1	04/04/08	< 0.1	0.3456557
	20080870100	Abs 071607LC: 50 µl	0.1	04/04/08	< 0.1	0.3439927
	20081290004	Abs 071607LC: 50 µl	0.1	05/16/08	< 0.1	0.3390336
	20081500007	Accu B7070230: 50 µl	0.1	06/19/08	< 0.1	0.3448469
	20083040065	ChemService 406-113B: 50 µl	0.1	11/19/08	< 0.1	0.5393643
	20083440101	Abs 081508Polar: 30 µl	0.1	12/30/08	< 0.1	0.3344064
	20091060131	Abs 081508Polar: 30 µl	0.1	04/30/09	< 0.1	0.3347432
	20091410005	ChemService 406-113B: 50 µl	0.1	06/17/09	< 0.1	0.5507839
	20091830170	Abs 081508Polar: 30 µl	0.1	07/28/09	< 0.1	0.330155
	20092530081	ChemService 406-113B: 30 µl	0.1	09/23/09	< 0.1	0.329352
	20093100008	Restek A069890: 40 µl	0.1	11/20/09	< 0.1	0.1842234
	20100920050	Restek A069890: 40 µl	0.1	04/14/10	< 0.1	0.1880564
	20101270033	Spex Organics T1090828008: 40 µl	0.1	05/26/10	< 0.1	0.1907467
	20101550008	Restek A069890: 80 µl	0.1	06/16/10	< 0.1	0.3845367
	20101760005	Restek A069890: 40 µl	0.1	07/14/10	< 0.1	0.1879248
	20103430088	ChemService 448-45B: 40 µl	0.1	01/04/11	< 0.1	0.1450068
	20110130055	Abs 090910HPLC: 40 µl	0.1	02/02/11	< 0.1	0.1506629
	20110410063	Abs 090910HPLC: 40 µl	0.1	02/25/11	< 0.1	0.1494322
	20110490034	ChemService 448-45B: 40 µl	0.1	03/07/11	< 0.1	0.1443439
	20110770004	Abs 090910HPLC: 40 µl	0.1	04/12/11	< 0.1	0.1490757
	20111590002	ChemService 448-45B: 100 µl	0.1	06/28/11	< 0.1	0.3669634
False Positive	20093380008	NSI 090309-01HPLC: 80 µl	0.1	12/29/09	E 0.019	0
	20101340151	Accu 209081166: 80 µl	0.1	06/10/10	E 0.062	0
	20111960035	Crescent 163162: 100 µl	0.1	07/18/11	. 0.087	0

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

CLOPYRALID

Schedule: 2060 Testid: 49305LCM29

Link to Individual Chart

False Positive & Negative Listing for CLOPYRALID

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20072140017	Supelco LB40676: 50 µl	0.06	08/23/07	< 0.06	0.0848953
	20080290026	Crescent 07GG007: 50 µl	0.06	02/12/08	< 0.06	0.1583087
	20092960006	Crescent 08LL073: 40 µl	0.06	11/20/09	< 0.06	0.0754942
	20101480008	Crescent 08LL073: 40 µl	0.06	06/17/10	< 0.06	0.0788136
	20101950136	Crescent 08LL073: 40 µl	0.06	07/28/10	< 0.06	0.0752252

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

CYCLOATE

Schedule: 2060 Testid: 04031LCM29

Link to Individual Chart

False Positive & Negative Listing for CYCLOATE

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Positive	20093520062	Spex Organics T1090828008: 40 µl	0.04	12/30/09	E 0.006	0

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

DACTHAL MONOACID

Schedule: 2060 Testid: 49304LCM29

Link to Individual Chart

False Positive & Negative Listing for DACTHAL MONOACID

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20071290015	Restek A046748: 75 µl	0.02	06/02/07	< 0.02	0.0701562
	20092820001	Accu 209081166: 40 µl	0.04	10/21/09	< 0.04	0.0510973
	20103020153	Crescent 163162: 40 µl	0.04	11/30/10	< 0.04	0.0514851
	20121810017	Spex Organics T1120525009: 50 µl & Supelco LB92941: 50 µl	0.04	07/20/12	< 0.04	0.375
	20122300023	Spex Organics T1120525009: 20 µl & NSI 062612-01: 20 µl & NSI 718L-01-01: 20 µl	0.04	09/15/12	< 0.04	0.15
	20123490150	Spex Organics T1120525009: 50 µl & Restek A088383: 50 µl	0.04	12/21/12	< 0.04	0.375

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

DEISOPROPYLATRAZINE (2-CHLORO-6-ETHYLAMINO-4-AMINO-S-TRIAZINE) CEAT

Schedule: 2060 Testid: 04038LCM29

Link to Individual Chart

False Positive & Negative Listing for DEISOPROPYLATRAZINE (2-CHLORO-6-ETHYLAMINO-4-AMINO-S-TRIAZINE) CEAT

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20102630167	Crescent 08LL073: 80 µl	0.06	10/28/10	< 0.06	0.1592198

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

DICAMBA

Schedule: 2060 Testid: 38442LCM29

Link to Individual Chart

False Positive & Negative Listing for DICAMBA

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20072900076	Abs 071607LC: 50 µl	0.04	11/06/07	< 0.04	0.279338
	20080150157	Accu B7070230: 50 µl	0.04	02/12/08	< 0.04	0.2843157
	20092400046	Supelco LB60726: 30 µl	0.04	09/30/09	< 0.04	0.1765857
	20092820001	Accu 209081166: 40 µl	0.04	10/21/09	< 0.04	0.0543254
	20093240039	ChemService 430-40B: 40 µl	0.04	12/03/09	< 0.04	0.0579885
	20100360001	Accu 209081166: 40 µl	0.04	02/18/10	< 0.04	0.0550294
	20101130051	ChemService 430-40B: 40 µl	0.04	05/05/10	< 0.04	0.0589681
	20101900003	Accu 209081166: 40 µl	0.04	07/28/10	< 0.04	0.0551834
	20103020153	Crescent 163162: 40 µl	0.04	11/30/10	< 0.04	0.0752475
	20110620084	Restek A075600: 40 µl	0.04	03/25/11	< 0.04	0.0745986
	20112170175	Restek A075600: 40 µl	0.04	09/06/11	< 0.04	0.0748
	20112870074	Crescent 163162: 40 µl	0.06	11/01/11	< 0.06	0.076

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

DINOSEB

Schedule: 2060 Testid: 49301LCM29

Link to Individual Chart

False Positive & Negative Listing for DINOSEB

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Positive	20080740019	Accu B7070230: 50 µl	0.04	04/04/08	E 0.001	0

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

FLUMETSULAM

Schedule: 2060 Testid: 61694LCM29

Link to Individual Chart

False Positive & Negative Listing for FLUMETSULAM

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20072900076	Abs 071607LC: 50 µl	0.06	11/06/07	< 0.168	0.1760281
	20092530081	ChemService 406-113B: 30 µl	0.06	09/23/09	< 0.06	0.0797253

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

FLUOMETURON

Schedule: 2060 Testid: 38811LCM29

Link to Individual Chart

False Positive & Negative Listing for FLUOMETURON

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20072200099	Accu B6070187: 75 µl	0.04	08/25/07	< 0.04	0.2042629

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

IMIDACLOPRID

Schedule: 2060 Testid: 61695LCM29

Link to Individual Chart

False Positive & Negative Listing for IMIDACLOPRID

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20080740019	Accu B7070230: 50 µl	0.06	04/04/08	< 0.06	0.1473078
	20082350002	Abs 071607LC: 50 µl	0.06	09/09/08	< 0.06	0.1428005

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

MCPB

Schedule: 2060 Testid: 38487LCM29

Link to Individual Chart

False Positive & Negative Listing for MCPB

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20113010045	Abs 090910HPLC: 40 µl	0.2	11/29/11	< 0.2	0.2512
	20120200070	ChemService 448-45B: 40 µl	0.2	02/03/12	< 0.2	0.2504
	20120690030	ChemService 448-45B: 40 µl	0.2	03/27/12	< 0.2	0.2504
	20120830076	Abs 090910HPLC: 40 µl	0.2	04/11/12	< 0.2	0.2512
	20121110019	Abs 090910HPLC: 40 µl	0.2	05/03/12	< 0.2	0.2512
	20122020005	NSI 062612-01: 20 µl & NSI 718L-01-01: 20 µl & ChemService 396400: 20 µl	0.2	08/08/12	< 0.2	0.25
	20122210007	Abs 052312: 20 µl & Restek A088383: 20 µl	0.2	08/23/12	< 0.2	0.25
	20122570123	NSI 062612-01: 20 µl & NSI 718L-01-01: 20 µl & Restek A088383: 20 µl	0.2	09/29/12	< 0.2	0.25
	20123260035	Supelco LB92941: 20 µl & ChemService 396400: 20 µl	0.2	12/06/12	< 0.2	0.25

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

METHIOCARB

Schedule: 2060 Testid: 38501LCM29

Link to Individual Chart

False Positive & Negative Listing for METHIOCARB

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20121460002	Crescent 163162: 40 µl	0.04	06/20/12	< 0.04	0.044

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

METSULFURON METHYL

Schedule: 2060 Testid: 61697LCM29

Link to Individual Chart

False Positive & Negative Listing for METSULFURON METHYL

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20101410004	Spex Organics T1090828008: 80 µl	0.14	06/11/10	< 0.14	0.4379853

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

NICOSULFURON

Schedule: 2060 Testid: 50364LCM29

Link to Individual Chart

False Positive & Negative Listing for NICOSULFURON

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20073110114	Accu B7070230: 50 µl	0.1	11/28/07	< 0.1	0.1481026
	20080150157	Accu B7070230: 50 µl	0.1	02/12/08	< 0.1	0.1480267
	20080370106	Abs 071607LC: 50 µl	0.1	02/12/08	< 0.1	0.1481294
	20080740019	Accu B7070230: 50 µl	0.1	04/04/08	< 0.1	0.1472568
	20080870100	Abs 071607LC: 50 µl	0.1	04/04/08	< 0.1	0.1477857
	20081290004	Abs 071607LC: 50 µl	0.1	05/16/08	< 0.1	0.1456552
	20081500007	Accu B7070230: 50 µl	0.1	06/19/08	< 0.1	0.1469122
	20081780159	Abs 071607LC: 50 µl	0.1	07/09/08	< 0.1	0.1446771
	20082000011	Accu B7070230: 50 µl	0.1	07/30/08	< 0.1	0.1412778
	20082350002	Abs 071607LC: 50 µl	0.1	09/09/08	< 0.1	0.1452797
	20082480185	Accu B7070230: 50 µl	0.1	09/25/08	< 0.1	0.1418328
	20082560003	Accu B7070230: 50 µl	0.1	09/25/08	< 0.1	0.1423782
	20112310031	Abs 090910HPLC: 100 µl	0.1	09/12/11	< 0.1	0.273

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

ORYZALIN

Schedule: 2060 Testid: 49292LCM29

Link to Individual Chart

False Positive & Negative Listing for ORYZALIN

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20080940065	Restek A053251: 50 µl	0.04	04/30/08	< 0.04	0.0708229

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

OXAMYL

Schedule: 2060 Testid: 38866LCM29

Link to Individual Chart

False Positive & Negative Listing for OXAMYL

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Positive	20092960006	Crescent 08LL073: 40 µl	0.12	11/19/09	E 0.002	0

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

PICLORAM

Schedule: 2060 Testid: 49291LCM29

Link to Individual Chart

False Positive & Negative Listing for PICLORAM

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20071290015	Restek A046748: 75 µl	0.12	06/02/07	< 0.12	0.2216638
	20072900076	Abs 071607LC: 50 µl	0.12	11/06/07	< 0.12	0.3891675
	20080150157	Accu B7070230: 50 µl	0.12	02/12/08	< 0.12	0.4016402
	20080370106	Abs 071607LC: 50 µl	0.12	02/12/08	< 0.12	0.3923155
	20080740019	Accu B7070230: 50 µl	0.12	04/04/08	< 0.12	0.3995513
	20080870100	Abs 071607LC: 50 µl	0.12	04/04/08	< 0.12	0.3914052
	20082000011	Accu B7070230: 50 µl	0.12	07/31/08	< 0.12	0.3833285
	20100920050	Restek A069890: 40 µl	0.12	04/14/10	< 0.12	0.2576773
	20101550008	Restek A069890: 80 µl	0.12	06/17/10	< 0.12	0.5268971
False Positive	20080240003	Protocol I1070803003: 50 µl	0.12	02/12/08	E 0.094	0
	20100630038	Crescent 08LL073: 40 µl	0.12	03/18/10	E 0.016	0

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

PROPHAM

Schedule: 2060 Testid: 49236LCM29

Link to Individual Chart

False Positive & Negative Listing for PROPHAM

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20072400295	Restek A046748: 50 µl	0.06	09/12/07	< 0.06	0.0700238

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

TERBACIL

Schedule: 2060 Testid: 04032LCM29

Link to Individual Chart

False Positive & Negative Listing for TERBACIL

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Positive	20120200070	ChemService 448-45B: 40 µl	0.046	02/02/12	. 0.003	0

Updated 06/06/2013