SAS Output

BQS Organic Blind Sample Project

False Positive and Negative Report for

Schedule: 1383

Analyte	TestIDCode	CASNumber	# Samples Spiked	# False Negatives	# Samples Not Spiked	# False Positives
1,2,4-TRICHLOROBENZENE	34551GCM57	120-82-1	57	2	83	4
1,2-DICHLOROBENZENE	34536GCM57	95-50-1	58	2	82	1
1,2-DIPHENYLHYDRAZINE	82626GCM55	122-66-7	52	1	88	4
1,3-DICHLOROBENZENE	34566GCM57	541-73-1	58	2	82	0
1,4-DICHLOROBENZENE	34571GCM57	106-46-7	58	2	82	0
2,4,6-TRICHLOROPHENOL	34621GCM56	88-06-2	52	0	88	3
2,4-DICHLOROPHENOL	34601GCM56	120-83-2	54	1	86	0
2,4-DIMETHYLPHENOL	34606GCM56	105-67-9	54	0	86	1
2,4-DINITROPHENOL	34616GCM56	51-28-5	54	4	86	0
2,4-DINITROTOLUENE	34611GCM57	121-14-2	54	0	86	0
2,6-DINITROTOLUENE	34626GCM57	606-20-2	54	1	86	1
2-CHLORONAPHTHALENE	34581GCM57	91-58-7	57	1	83	0
2-CHLOROPHENOL	34586GCM56	95-57-8	54	1	86	1
2-NITROPHENOL	34591GCM56	88-75-5	52	3	88	1
3,3DICHLOROBENZIDINE	34631GCM55	91-94-1	54	8	86	0
4,6-DINITRO-2-METHYLPHENOL	34657GCM56	534-52-1	54	1	86	0
4-BROMOPHENYLPHENYLETHER	34636GCM57	101-55-3	57	2	83	1
4-CHLORO-3-METHYLPHENOL	34452GCM56	59-50-7	45	0	95	1
4-CHLOROPHENYL PHENYL ETHER	34641GCM57	7005-72-3	55	1	85	1
4-NITROPHENOL	34646GCM56	100-02-7	54	2	86	0
ACENAPHTHENE	34205GCM57	83-32-9	56	1	84	0
ACENAPHTHYLENE	34200GCM57	208-96-8	56	1	84	1
ANTHRACENE	34220GCM57	120-12-7	58	1	82	3
BENZIDINE	39120GCM55	92-87-5	0	0	153	0
BENZO[A]PYRENE	34247GCM57	50-32-8	56	1	84	2
BENZO[B]FLUORANTHENE	34230GCM57	205-99-2	55	1	85	3
BENZO[GHI]PERYLENE	34521GCM57	191-24-2	54	0	86	2
BENZO[K]FLUORANTHENE	34242GCM57	207-08-9	55	1	85	1
BENZ[A]ANTHRACENE	34526GCM57	56-55-3	55	1	85	1
BIS(2-CHLOROETHOXY)METHANE	34278GCM57	111-91-1	51	1	89	0
BIS(2-CHLOROETHYL)ETHER	34273GCM57	111-44-4	56	2	84	0
BIS(2-CHLOROISOPROPYL) ETHER	34283GCM57	108-60-1	57	2	83	0
BIS(2-ETHYLHEXYL) PHTHALATE	39100GCM57	117-81-7	50	4	90	5
BUTYLBENZYL PHTHALATE	34292GCM57	85-68-7	54	0	86	2
CHRYSENE	34320GCM57	218-01-9	56	1	84	1
DI-N-BUTYL PHTHALATE	39110GCM57	84-74-2	54	0	86	1
DI-N-OCTYL PHTHALATE	34596GCM57	117-84-0	54	0	86	0
DIBENZ[A,H]ANTHRACENE	34556GCM57	53-70-3	54	0	86	0
DIETHYL PHTHALATE	34336GCM57	84-66-2	54	0	86	1
DIMETHYL PHTHALATE	34341GCM57	131-11-3	55	1	85	3
FLUORANTHENE	34376GCM57	206-44-0	56	1	84	2
FLUORENE	34381GCM57	86-73-7	56	1	84	4
HEXACHLOROBENZENE	39700GCM57	118-74-1	56	1	84	1
HEXACHLOROBUTADIENE	39702GCM57	87-68-3	57	2	83	15
HEXACHLOROCYCLOPENTADIENE	34386GCM57	77-47-4	54	0	86	0
HEXACHLOROETHANE	34396GCM57	67-72-1	57	1	83	3
INDENO[1,2,3-CD]PYRENE	34403GCM57	193-39-5	54	0	86	1
ISOPHORONE	34408GCM57	78-59-1	54	0	86	0
N-NITROSODI-N-PROPYLAMINE	34428GCM57	621-64-7	54	2	86	0
N-NITROSODIMETHYLAMINE	34438GCM57	62-75-9	56	1	84	0
N-NITROSODIPHENYLAMINE	34433GCM57	86-30-6	54	3	86	1
NAPHTHALENE	34696GCM57	91-20-3	55	1	85	1
NITROBENZENE	34447GCM57	98-95-3	55	1	85	2
PENTACHLOROPHENOL	39032GCM56	87-86-5	54	0	86	0
PHENANTHRENE	34461GCM57	85-01-8	56	1	84	1
PHENOL	34694GCM56	108-95-2	54	1	86	1
PYRENE	34469GCM57	129-00-0	56	1	84	4

BQS Organic Blind Sample Program

False Positives & False Negatives

1,2,4-TRICHLOROBENZENE

Schedule: 1383 Testid: 34551GCM57

Link to Individual Chart

False Positive & Negative Listing for 1,2,4-TRICHLOROBENZENE

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20072070014	ERA 0714-06-02: 25 µl	0.41	08/27/07	< 0.41	1.57596
	20121310030	Crescent 06MM151: 80 µl	0.26	07/12/12	< 0.26	0.6719999
False Positive	20071220020	Ultra CC-2390: 50 µl	0.41	06/07/07	E 0.0042	0
	20071440019	Supelco LB40675: 50 µl	0.41	06/07/07	E 0.0032	0
	20071500019	Ultra CC-2390: 25 µl	0.41	06/07/07	E 0.0059	0
	20090430169	Accu B8090087: 40 µl	0.2	03/10/09	E 0.0052	0

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

1,2-DICHLOROBENZENE

Schedule: 1383 Testid: 34536GCM57

Link to Individual Chart

False Positive & Negative Listing for 1,2-DICHLOROBENZENE

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20072070014	ERA 0714-06-02: 25 µl	0.49	08/27/07	< 0.49	1.839465
	20121310030	Crescent 06MM151: 80 µl	0.2	07/12/12	< 0.2	0.744
False Positive	20090430169	Accu B8090087: 40 µl	0.2	03/10/09	E 0.0038	0

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

1,2-DIPHENYLHYDRAZINE

Schedule: 1383 Testid: 82626GCM55

Link to Individual Chart

False Positive & Negative Listing for 1,2-DIPHENYLHYDRAZINE

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20121310030	Crescent 06MM151: 80 µl	0.3	07/12/12	< 0.3	0.648
False Positive	20090580006	Restek A062189: 25 µl	0.3	03/13/09	E 1.5	0
	20091320005	Restek A062189: 25 µl	0.3	08/04/09	. 1.67	0
	20091700147	Restek A062189: 40 µl	0.3	08/25/09	. 2.32	0
	20092110203	Restek A062189: 25 µl	0.3	09/22/09	. 1.3	0

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

1,3-DICHLOROBENZENE

Schedule: 1383 Testid: 34566GCM57

Link to Individual Chart

False Positive & Negative Listing for 1,3-DICHLOROBENZENE

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20072070014	ERA 0714-06-02: 25 µl	0.57	08/27/07	< 0.57	0.940002
	20121310030	Crescent 06MM151: 80 µl	0.22	07/12/12	< 0.22	1.488

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

1,4-DICHLOROBENZENE

Schedule: 1383 Testid: 34571GCM57

Link to Individual Chart

False Positive & Negative Listing for 1,4-DICHLOROBENZENE

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20072070014	ERA 0714-06-02: 25 µl	0.53	08/27/07	< 0.53	2.044694
	20121310030	Crescent 06MM151: 80 µl	0.22	07/12/12	< 0.22	1.504

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

2,4,6-TRICHLOROPHENOL

Schedule: 1383 Testid: 34621GCM56

Link to Individual Chart

False Positive & Negative Listing for 2,4,6-TRICHLOROPHENOL

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
False Positive	20090430169	Accu B8090087: 40 µl	0.6	03/10/09	E 0.0554
	20090860040	Accu B8090087: 25 µl	0.6	04/28/09	E 0.0167
	20100990015	Ultra CF-3574: 80 µl	0.34	05/13/10	E 0.013

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

2,4-DICHLOROPHENOL

Schedule: 1383 Testid: 34601GCM56

Link to Individual Chart

False Positive & Negative Listing for 2,4-DICHLOROPHENOL

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20072070014	ERA 0714-06-02: 25 µl	0.39	08/27/07	< 0.39	0.6384919

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

2,4-DIMETHYLPHENOL

Schedule: 1383 Testid: 34606GCM56

Link to Individual Chart

False Positive & Negative Listing for 2,4-DIMETHYLPHENOL

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Positive	20080870098	Supelco LB50016: 40 µl	0.6	04/07/08	E 0.147	0

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

2,4-DINITROPHENOL

Schedule: 1383 Testid: 34616GCM56

Link to Individual Chart

False Positive & Negative Listing for 2,4-DINITROPHENOL

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20070950016	Supelco LB40675: 25 µl	0.8	04/28/07	< 0.8	1.493899
	20073310066	ERA 0709-07-03BNA: 25 µl	0.8	02/01/08	< 0.8	1.746184
	20090500128	ChemService 406-96B: 25 µl	1.4	03/10/09	< 1.4	2.840331
	20101550009	Supelco LB69646: 40 µl	1.4	06/15/10	< 1.4	2.249772

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

2,6-DINITROTOLUENE

Schedule: 1383 Testid: 34626GCM57

Link to Individual Chart

False Positive & Negative Listing for 2,6-DINITROTOLUENE

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20072070014	ERA 0714-06-02: 25 µl	0.43	08/27/07	< 0.43	1.345394
False Positive	20100990015	Ultra CF-3574: 80 µl	0.4	05/13/10	E 0.03	0

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

2-CHLORONAPHTHALENE

Schedule: 1383 Testid: 34581GCM57

Link to Individual Chart

False Positive & Negative Listing for 2-CHLORONAPHTHALENE

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20121310030	Crescent 06MM151: 80 µl	0.24	07/12/12	< 0.24	0.696

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

2-CHLOROPHENOL

Schedule: 1383 Testid: 34586GCM56

Link to Individual Chart

False Positive & Negative Listing for 2-CHLOROPHENOL

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20072070014	ERA 0714-06-02: 25 µl	0.42	08/27/07	< 0.42	0.9476031
False Positive	20090430169	Accu B8090087: 40 µl	0.42	03/10/09	E 0.0102	0

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

2-NITROPHENOL

Schedule: 1383 Testid: 34591GCM56

Link to Individual Chart

False Positive & Negative Listing for 2-NITROPHENOL

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20122230021	Restek A088363: 20 µl & NSI 060612-01: 20 µl	0.4	08/18/12	< 0.4	2
	20122720047	ERA 0507-12-03.1: 50 µl & NSI 060612-01: 50 µl	0.4	10/26/12	< 0.4	5
	20123490151	ERA 0507-12-03.1: 100 µl & NSI 060612-01: 100 µl	0.4	01/08/13	< 0.4	10
False Positive	20071220020	Ultra CC-2390: 50 µl	0.3	06/07/07	E 0.0305	0

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

3,3DICHLOROBENZIDINE

Schedule: 1383 Testid: 34631GCM55

Link to Individual Chart

False Positive & Negative Listing for 3,3DICHLOROBENZIDINE

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20071220020	Ultra CC-2390: 50 µl	0.65	06/07/07	< 0.65	0.8391746
	20071440019	Supelco LB40675: 50 µl	0.65	06/07/07	< 0.65	0.8300532
	20091620173	ChemService 406-96B: 25 µl	0.4	08/25/09	< 0.4	1.304261
	20120620016	Spex Organics T1100701002: 50 µl	0.42	03/20/12	< 0.42	0.8649999
	20121950067	ERA 0507-12-03.1: 20 µl & Supelco LB92780: 20 µl	0.42	08/10/12	< 0.42	0.4996
	20122230021	Restek A088363: 20 µl & NSI 060612-01: 20 µl	0.42	08/18/12	< 0.42	0.5
	20122720047	ERA 0507-12-03.1: 50 µl & NSI 060612-01: 50 µl	0.42	10/26/12	< 0.42	1.25
	20123490151	ERA 0507-12-03.1: 100 µl & NSI 060612-01: 100 µl	0.42	01/08/13	< 0.42	2.5

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

4,6-DINITRO-2-METHYLPHENOL

Schedule: 1383 Testid: 34657GCM56

Link to Individual Chart

False Positive & Negative Listing for 4,6-DINITRO-2-METHYLPHENOL

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20091410006	Abs 080508BNA: 25 µl	0.77	07/07/09	< 0.77	1.025127

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

4-BROMOPHENYLPHENYLETHER

Schedule: 1383 Testid: 34636GCM57

Link to Individual Chart

False Positive & Negative Listing for 4-BROMOPHENYLPHENYLETHER

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20072070014	ERA 0714-06-02: 25 µl	0.36	08/27/07	< 0.36	1.066687
	20121310030	Crescent 06MM151: 80 µl	0.24	07/12/12	< 0.24	0.92
False Positive	20100990015	Ultra CF-3574: 80 µl	0.24	05/13/10	E 0.018	0

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

4-CHLORO-3-METHYLPHENOL

Schedule: 1383 Testid: 34452GCM56

Link to Individual Chart

False Positive & Negative Listing for 4-CHLORO-3-METHYLPHENOL

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Positive	20100990015	Ultra CF-3574: 80 µl	0.55	05/13/10	E 0.021	0

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

4-CHLOROPHENYL PHENYL ETHER

Schedule: 1383 Testid: 34641GCM57

Link to Individual Chart

False Positive & Negative Listing for 4-CHLOROPHENYL PHENYL ETHER

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20121310030	Crescent 06MM151: 80 µl	0.34	07/12/12	< 0.34	1.512
False Positive	20100990015	Ultra CF-3574: 80 µl	0.34	05/13/10	E 0.016	0

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

4-NITROPHENOL

Schedule: 1383 Testid: 34646GCM56

Link to Individual Chart

False Positive & Negative Listing for 4-NITROPHENOL

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20072070014	ERA 0714-06-02: 25 µl	0.51	08/27/07	< 0.51	2.290463
	20091410006	Abs 080508BNA: 25 µl	0.51	07/07/09	< 0.51	0.8420513

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

ACENAPHTHENE

Schedule: 1383 Testid: 34205GCM57

Link to Individual Chart

False Positive & Negative Listing for ACENAPHTHENE

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20121310030	Crescent 06MM151: 80 µl	0.28	07/12/12	< 0.28	0.752

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

ACENAPHTHYLENE

Schedule: 1383 Testid: 34200GCM57

Link to Individual Chart

False Positive & Negative Listing for ACENAPHTHYLENE

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20121310030	Crescent 06MM151: 80 µl	0.3	07/12/12	< 0.3	0.816
False Positive	20070800008	Restek A046609: 50 µl	0.3	04/28/07	E 0.0142	0

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

ANTHRACENE

Schedule: 1383 Testid: 34220GCM57

Link to Individual Chart

False Positive & Negative Listing for ANTHRACENE

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20121310030	Crescent 06MM151: 80 µl	0.38	07/12/12	< 0.38	1.408
False Positive	20070580110	ChemService 363-135A: 50 µl	0.39	04/13/07	E 0.015	0
	20103020154	Spex Organics T1100701002: 80 µl	0.38	12/07/10	. 0.003	0
	20103510061	Spex Organics T1100701002: 200 µl	0.38	01/25/11	. 0.004	0

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

BENZO[A]PYRENE

Schedule: 1383 Testid: 34247GCM57

Link to Individual Chart

False Positive & Negative Listing for BENZO[A]PYRENE

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20121310030	Crescent 06MM151: 80 µl	0.32	07/12/12	< 0.32	0.872
False Positive	20070950016	Supelco LB40675: 25 µl	0.33	04/28/07	E 0.0271	0
	20103510061	Spex Organics T1100701002: 200 µl	0.32	01/25/11	. 0.006	0

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

BENZO[B]FLUORANTHENE

Schedule: 1383 Testid: 34230GCM57

Link to Individual Chart

False Positive & Negative Listing for BENZO[B]FLUORANTHENE

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20072070014	ERA 0714-06-02: 25 µl	0.4	08/27/07	< 0.4	2.052295
False Positive	20070950016	Supelco LB40675: 25 µl	0.4	04/28/07	E 0.052	0
	20071010008	ChemService 363-135A: 25 µl	0.4	04/28/07	E 0.0109	0
	20071440019	Supelco LB40675: 50 µl	0.4	06/07/07	E 0.0044	0

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

BENZO[GHI]PERYLENE

Schedule: 1383 Testid: 34521GCM57

Link to Individual Chart

False Positive & Negative Listing for BENZO[GHI]PERYLENE

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Positive	20073060020	Supelco LB50016: 25 µl	0.4	01/16/08	E 0.0602	0
	20100990015	Ultra CF-3574: 80 µl	0.38	05/13/10	E 0.029	0

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

BENZO[K]FLUORANTHENE

Schedule: 1383 Testid: 34242GCM57

Link to Individual Chart

False Positive & Negative Listing for BENZO[K]FLUORANTHENE

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20072070014	ERA 0714-06-02: 25 µl	0.45	08/27/07	< 0.45	0.7170365
False Positive	20070950016	Supelco LB40675: 25 µl	0.45	04/28/07	E 0.0231	0

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

BENZ[A]ANTHRACENE

Schedule: 1383 Testid: 34526GCM57

Link to Individual Chart

False Positive & Negative Listing for BENZ[A]ANTHRACENE

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20121310030	Crescent 06MM151: 80 µl	0.26	07/12/12	< 0.26	0.528
False Positive	20111190182	Supelco LB77169: 200 µl	0.26	05/17/11	. 0.007	0

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

BIS(2-CHLOROETHOXY)METHANE

Schedule: 1383 Testid: 34278GCM57

Link to Individual Chart

False Positive & Negative Listing for BIS(2-CHLOROETHOXY)METHANE

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20121310030	Crescent 06MM151: 80 µl	0.24	07/12/12	< 0.24	0.808

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

BIS(2-CHLOROETHYL)ETHER

Schedule: 1383 Testid: 34273GCM57

Link to Individual Chart

False Positive & Negative Listing for BIS(2-CHLOROETHYL)ETHER

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20091880134	NSI 080508-01BNA: 25 µl	0.3	09/01/09	< 0.3	1.083178
	20121310030	Crescent 06MM151: 80 µl	0.3	07/12/12	< 0.3	1.008

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

BIS(2-CHLOROISOPROPYL) ETHER

Schedule: 1383 Testid: 34283GCM57

Link to Individual Chart

False Positive & Negative Listing for BIS(2-CHLOROISOPROPYL) ETHER

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20072070014	ERA 0714-06-02: 25 µl	0.38	08/27/07	< 0.38	0.6993007
	20121310030	Crescent 06MM151: 80 µl	0.14	07/12/12	< 0.14	1

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

BIS(2-ETHYLHEXYL) PHTHALATE

Schedule: 1383 Testid: 39100GCM57

Link to Individual Chart

False Positive & Negative Listing for BIS(2-ETHYLHEXYL) PHTHALATE

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20080370104	ERA 0709-07-03BNA: 25 µl	2	02/22/08	< 3.75	3.795967
	20091410006	Abs 080508BNA: 25 µl	2	07/07/09	< 2	3.897634
	20091830167	Abs 080508BNA: 25 µl	2	09/01/09	< 2	3.883585
	20101550009	Supelco LB69646: 40 µl	2	06/15/10	< 2.8	4.703257
False Positive	20090430169	Accu B8090087: 40 µl	2	03/10/09	E 0.484	0
	20093240043	ERA 0817-09-02BNA: 80 µl	2	01/26/10	E 0.7	0
	20093380007	Crescent 08LL068: 40 µl	2	01/28/10	. 3.5	0
	20112310033	Crescent 06MM151: 80 µl	2.6	09/16/11	E 0.26	0
	20113220199	Crescent 06MM151: 50 µl	7.2	01/10/12	E 4.92	0

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

BUTYLBENZYL PHTHALATE

Schedule: 1383 Testid: 34292GCM57

Link to Individual Chart

False Positive & Negative Listing for BUTYLBENZYL PHTHALATE

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Positive	20102880002	Crescent 06MM151: 50 µl	1.8	12/02/10	. 0.81	0
	20103350002	ERA 0618-10-02 LS1383#1: 80 µl	1.8	01/25/11	. 0.41	0

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

CHRYSENE

Schedule: 1383 Testid: 34320GCM57

Link to Individual Chart

False Positive & Negative Listing for CHRYSENE

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20121310030	Crescent 06MM151: 80 µl	0.32	07/12/12	< 0.32	1.544
False Positive	20070950016	Supelco LB40675: 25 µl	0.33	04/28/07	E 0.0313	0

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

DI-N-BUTYL PHTHALATE

Schedule: 1383 Testid: 39110GCM57

Link to Individual Chart

False Positive & Negative Listing for DI-N-BUTYL PHTHALATE

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Positive	20110070108	Crescent 06MM151: 50 µl	2	01/25/11	. 0.1	0

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

DIETHYL PHTHALATE

Schedule: 1383 Testid: 34336GCM57

Link to Individual Chart

False Positive & Negative Listing for DIETHYL PHTHALATE

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Positive	20082260237	Supelco LB50016: 25 µl	0.61	08/20/08	E 0.637	0

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

DIMETHYL PHTHALATE

Schedule: 1383 Testid: 34341GCM57

Link to Individual Chart

False Positive & Negative Listing for DIMETHYL PHTHALATE

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20102250099	ERA 0817-09-02BNA: 40 µl	0.36	10/19/10	< 0.36	0.6403891
False Positive	20111390174	ERA 0618-10-02 LS1383#1: 50 µl	0.36	06/07/11	. 0.032	0
	20112170173	ERA 0618-10-02 LS1383#1: 200 µl	0.36	09/15/11	E 0.017	0
	20112310033	Crescent 06MM151: 80 µl	0.36	09/16/11	E 0.022	0

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

FLUORANTHENE

Schedule: 1383 Testid: 34376GCM57

Link to Individual Chart

False Positive & Negative Listing for FLUORANTHENE

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20121310030	Crescent 06MM151: 80 µl	0.3	07/12/12	< 0.3	1.312
False Positive	20070950016	Supelco LB40675: 25 µl	0.3	04/28/07	E 0.097	0
	20103510061	Spex Organics T1100701002: 200 µl	0.3	01/25/11	. 0.008	0

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

FLUORENE

Schedule: 1383 Testid: 34381GCM57

Link to Individual Chart

False Positive & Negative Listing for FLUORENE

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20121310030	Crescent 06MM151: 80 µl	0.34	07/12/12	< 0.34	1.112
False Positive	20091700147	Restek A062189: 40 µl	0.33	08/25/09	E 0.0076	0
	20092110203	Restek A062189: 25 µl	0.33	09/22/09	E 0.0043	0
	20100990015	Ultra CF-3574: 80 µl	0.33	05/13/10	E 0.025	0
	20101720150	Ultra CF-3574: 40 µl	0.33	07/15/10	E 0.005	0

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

HEXACHLOROBENZENE

Schedule: 1383 Testid: 39700GCM57

Link to Individual Chart

False Positive & Negative Listing for HEXACHLOROBENZENE

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20121310030	Crescent 06MM151: 80 µl	0.3	07/12/12	< 0.3	1.016
False Positive	20090430169	Accu B8090087: 40 µl	0.3	03/10/09	E 0.0498	0

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

HEXACHLOROBUTADIENE

Schedule: 1383 Testid: 39702GCM57

Link to Individual Chart

False Positive & Negative Listing for HEXACHLOROBUTADIENE

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20072070014	ERA 0714-06-02: 25 µl	0.46	08/27/07	< 0.46	1.745718
	20121310030	Crescent 06MM151: 80 µl	0.24	07/12/12	< 0.24	1.152
False Positive	20090430169	Accu B8090087: 40 µl	0.2	03/10/09	E 0.0107	0
	20090640120	Ultra CE-2870: 25 µl	0.2	03/13/09	E 0.0178	0
	20090860040	Accu B8090087: 25 µl	0.2	04/28/09	E 0.0162	0
	20091340059	Ultra CE-2870: 25 µl	0.2	08/04/09	E 0.0141	0
	20091550182	Accu B8090087: 25 µl	0.2	07/14/09	E 0.0137	0
	20091770123	Ultra CE-2870: 40 µl	0.2	07/14/09	E 0.0201	0
	20091970070	Accu B8090087: 25 µl	0.2	09/15/09	E 0.0195	0
	20092260007	Ultra CE-2870: 25 µl	0.24	10/06/09	E 0.0157	0
	20101130053	ERA 0817-09-02BNA: 40 µl	0.24	06/10/10	E 0.002	0
	20103020154	Spex Organics T1100701002: 80 µl	0.24	12/07/10	. 0.004	0
	20103140136	Supelco LB77169: 50 µl	0.24	12/08/10	. 0.002	0
	20103510061	Spex Organics T1100701002: 200 µl	0.24	01/25/11	. 0.011	0
	20111190182	Supelco LB77169: 200 µl	0.24	05/17/11	. 0.007	0
	20111540002	Spex Organics T1100701002: 80 µl	0.24	06/23/11	. 0.003	0
	20111810001	Spex Organics T1100701002: 200 µl	0.24	07/15/11	. 0.012	0

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

HEXACHLOROETHANE

Schedule: 1383 Testid: 34396GCM57

Link to Individual Chart

False Positive & Negative Listing for HEXACHLOROETHANE

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20121310030	Crescent 06MM151: 80 µl	0.24	07/12/12	< 0.24	1.328
False Positive	20070800008	Restek A046609: 50 µl	0.66	04/28/07	E 0.0297	0
	20071360128	Restek A046609: 25 µl	0.66	06/07/07	E 0.0124	0
	20073190235	Ultra CD-2093: 25 µl	0.2	01/16/08	E 0.0155	0

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

INDENO[1,2,3-CD]PYRENE

Schedule: 1383 Testid: 34403GCM57

Link to Individual Chart

False Positive & Negative Listing for INDENO[1,2,3-CD]PYRENE

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Positive	20073060020	Supelco LB50016: 25 µl	0.4	01/16/08	E 0.123	0

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

N-NITROSODI-N-PROPYLAMINE

Schedule: 1383 Testid: 34428GCM57

Link to Individual Chart

False Positive & Negative Listing for N-NITROSODI-N-PROPYLAMINE

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20071220020	Ultra CC-2390: 50 µl	0.82	06/07/07	< 0.82	1.638859
	20121950067	ERA 0507-12-03.1: 20 µl & Supelco LB92780: 20 µl	0.4	08/10/12	< 0.88	1

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

N-NITROSODIMETHYLAMINE

Schedule: 1383 Testid: 34438GCM57

Link to Individual Chart

False Positive & Negative Listing for N-NITROSODIMETHYLAMINE

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20121310030	Crescent 06MM151: 80 µl	0.32	07/12/12	< 0.32	0.56

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

N-NITROSODIPHENYLAMINE

Schedule: 1383 Testid: 34433GCM57

Link to Individual Chart

False Positive & Negative Listing for N-NITROSODIPHENYLAMINE

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20071220020	Ultra CC-2390: 50 µl	0.81	06/07/07	< 0.81	1.910356
	20071500019	Ultra CC-2390: 25 µl	0.81	06/07/07	< 0.81	0.9435342
	20072350246	Ultra CC-2390: 25 µl	0.4	10/15/07	< 0.81	0.9488085
False Positive	20100990015	Ultra CF-3574: 80 µl	0.28	05/13/10	E 0.013	0

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

NAPHTHALENE

Schedule: 1383 Testid: 34696GCM57

Link to Individual Chart

False Positive & Negative Listing for NAPHTHALENE

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20121310030	Crescent 06MM151: 80 µl	0.22	07/12/12	< 0.22	0.712
False Positive	20112220130	Spex Organics T1100701002: 50 µl	0.22	09/16/11	. 0.132	0

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

NITROBENZENE

Schedule: 1383 Testid: 34447GCM57

Link to Individual Chart

False Positive & Negative Listing for NITROBENZENE

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20121310030	Crescent 06MM151: 80 µl	0.26	07/12/12	< 0.26	0.928
False Positive	20122720047	ERA 0507-12-03.1: 50 µl & NSI 060612-01: 50 µl	0.26	10/26/12	. 4.32	0
	20123490151	ERA 0507-12-03.1: 100 µl & NSI 060612-01: 100 µl	0.26	01/08/13	. 8.17	0

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

PHENANTHRENE

Schedule: 1383 Testid: 34461GCM57

Link to Individual Chart

False Positive & Negative Listing for PHENANTHRENE

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20121310030	Crescent 06MM151: 80 µl	0.32	07/12/12	< 0.32	1.248
False Positive	20070950016	Supelco LB40675: 25 µl	0.32	04/28/07	E 0.0237	0

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

PHENOL

Schedule: 1383 Testid: 34694GCM56

Link to Individual Chart

False Positive & Negative Listing for PHENOL

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20072070014	ERA 0714-06-02: 25 µl	0.44	08/27/07	< 0.44	1.535421
False Positive	20081010089	ERA 0709-07-03BNA: 25 µl	0.44	05/08/08	E 0.0356	0

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

PYRENE

Schedule: 1383 Testid: 34469GCM57

Link to Individual Chart

False Positive & Negative Listing for PYRENE

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20121310030	Crescent 06MM151: 80 µl	0.36	07/12/12	< 0.36	1.208
False Positive	20070950016	Supelco LB40675: 25 µl	0.35	04/28/07	E 0.0671	0
	20100990015	Ultra CF-3574: 80 µl	0.35	05/13/10	E 0.016	0
	20103020154	Spex Organics T1100701002: 80 µl	0.36	12/07/10	. 0.005	0
	20103510061	Spex Organics T1100701002: 200 µl	0.36	01/25/11	. 0.011	0

Updated 06/06/2013