Organic Blind Sample Project
False Positive and Negative Report for
Method: 4434

Analyte TestIDCode CASNumber # Samples
Spiked		 # False
Negatives		 # Samples
Not Spiked		 # False
Positives
11-KETOTESTOSTERONE 64527GM005 564-35-2 15 1 30 0
17-ALPHA-ESTRADIOL 64528GM005 57-91-0 28 3 17 1
17-ALPHA-ETHYNYLESTRADIOL 64529GM005 57-63-6 27 6 18 2
17-BETA-ESTRADIOL 64530GM005 50-28-2 31 9 14 1
3-BETA-COPROSTANOL 64532GM005 360-68-9 28 7 17 0
4,4BISPHENOL_F 51294GM005 620-92-8 18 0 27 0
4-ANDROSTENE-3,17-DIONE 64533GM005 63-05-8 15 4 30 1
BISPHENOL_A 67305GM005 80-05-7 29 0 16 0
CHOLESTEROL 64534GM005 57-88-5 29 13 16 0
CIS-ANDROSTERONE 64535GM005 53-41-8 30 3 15 0
DIHYDROTESTOSTERONE 64544GM005 521-18-6 29 4 16 0
EPITESTOSTERONE 64537GM005 481-30-1 29 4 16 0
EQUILENIN 64538GM005 517-09-9 12 0 18 1
EQUILIN 64539GM005 474-86-2 26 8 19 0
ESTRIOL 64540GM005 50-27-1 29 2 16 0
ESTRONE 64541GM005 53-16-7 33 8 12 0
MESTRANOL 64542GM005 72-33-3 26 15 16 1
NORETHINDRONE 64531GM005 68-22-4 28 11 17 0
PROGESTERONE 64543GM005 57-83-0 33 8 12 0
TESTOSTERONE 64545GM005 58-22-0 20 3 22 2
TRANS-DIETHYLSTILBESTROL 64536GM005 56-53-1 33 7 12 0

back to table
Organic Blind Sample Program
False Positives & False Negatives
11-KETOTESTOSTERONE
Method: 4434 Testid: 64527GM005
Link to Individual Chart

newdate = 06/02/17 falseneg = -0.01 newdate = 12/13/17 CENC_VAL = 26.900 newdate = 12/13/17 CENC_VAL = 3.500 newdate = 12/11/17 CENC_VAL = 6.000 newdate = 08/30/17 CENC_VAL = 20.000 newdate = 07/26/17 CENC_VAL = 7.800 newdate = 07/13/17 CENC_VAL = 9.400 newdate = 06/02/17 CENC_VAL = 12.400 newdate = 03/15/17 CENC_VAL = 11.000 newdate = 02/01/17 CENC_VAL = 4.500 newdate = 01/13/17 CENC_VAL = 4.100 newdate = 12/29/16 CENC_VAL = 5.300 newdate = 12/05/16 CENC_VAL = 5.300 newdate = 06/24/16 CENC_VAL = 2.600 newdate = 03/18/16 CENC_VAL = 20.000 newdate = 12/13/17 REPORTING LEVEL = 2 newdate = 12/13/17 REPORTING LEVEL = 2 newdate = 12/13/17 REPORTING LEVEL = 2 newdate = 12/11/17 REPORTING LEVEL = 2 newdate = 12/11/17 REPORTING LEVEL = 2 newdate = 08/30/17 REPORTING LEVEL = 2 newdate = 08/30/17 REPORTING LEVEL = 2 newdate = 07/26/17 REPORTING LEVEL = 2 newdate = 07/26/17 REPORTING LEVEL = 2 newdate = 07/13/17 REPORTING LEVEL = 2 newdate = 07/13/17 REPORTING LEVEL = 2 newdate = 06/02/17 REPORTING LEVEL = 2 newdate = 06/02/17 REPORTING LEVEL = 2 newdate = 06/02/17 REPORTING LEVEL = 2 newdate = 06/02/17 REPORTING LEVEL = 2 newdate = 03/15/17 REPORTING LEVEL = 2 newdate = 03/15/17 REPORTING LEVEL = 2 newdate = 02/01/17 REPORTING LEVEL = 2 newdate = 02/01/17 REPORTING LEVEL = 2 newdate = 01/13/17 REPORTING LEVEL = 2 newdate = 01/13/17 REPORTING LEVEL = 2 newdate = 12/29/16 REPORTING LEVEL = 2 newdate = 12/29/16 REPORTING LEVEL = 2 newdate = 12/07/16 REPORTING LEVEL = 2 newdate = 12/07/16 REPORTING LEVEL = 2 newdate = 12/05/16 REPORTING LEVEL = 2 newdate = 12/05/16 REPORTING LEVEL = 2 newdate = 06/24/16 REPORTING LEVEL = 2 newdate = 06/24/16 REPORTING LEVEL = 2 newdate = 03/18/16 REPORTING LEVEL = 2 Y = 0
The SGPlot Procedure

False Positive & Negative Listing for 11-KETOTESTOSTERONE

Status Lab ID Spike Mix Reporting Level Analysis Date Result Conc. Expected Conc.
False Negative 20170320040 Abs 052616: 50 µl & Abs 061416H: 50 µl 2 06/02/17 < 2 8.336842

Updated 03/28/2018

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Organic Blind Sample Program
False Positives & False Negatives
17-ALPHA-ESTRADIOL
Method: 4434 Testid: 64528GM005
Link to Individual Chart

newdate = 08/30/17 falseneg = -0.01 newdate = 07/12/16 falseneg = -0.01 newdate = 03/18/16 falseneg = -0.01 newdate = 08/31/16 falsepos = 10.2 newdate = 12/11/17 CENC_VAL = 10.300 newdate = 12/05/17 CENC_VAL = 7.430 newdate = 12/04/17 CENC_VAL = 0.930 newdate = 11/21/17 CENC_VAL = 1.380 newdate = 09/28/17 CENC_VAL = 3.370 newdate = 08/30/17 CENC_VAL = 4.210 newdate = 07/26/17 CENC_VAL = 3.820 newdate = 07/26/17 CENC_VAL = 1.560 newdate = 06/30/17 CENC_VAL = 5.280 newdate = 06/30/17 CENC_VAL = 3.480 newdate = 03/15/17 CENC_VAL = 4.450 newdate = 03/15/17 CENC_VAL = 1.590 newdate = 02/24/17 CENC_VAL = 2.230 newdate = 02/01/17 CENC_VAL = 1.820 newdate = 12/29/16 CENC_VAL = 1.860 newdate = 12/15/16 CENC_VAL = 3.330 newdate = 09/21/16 CENC_VAL = 1.740 newdate = 09/15/16 CENC_VAL = 1.780 newdate = 09/09/16 CENC_VAL = 2.110 newdate = 08/19/16 CENC_VAL = 8.470 newdate = 08/11/16 CENC_VAL = 5.670 newdate = 06/24/16 CENC_VAL = 1.990 newdate = 03/18/16 CENC_VAL = 0.960 newdate = 03/07/16 CENC_VAL = 1.080 newdate = 03/07/16 CENC_VAL = 1.090 newdate = 12/11/17 REPORTING LEVEL = 0.8 newdate = 12/05/17 REPORTING LEVEL = 0.8 newdate = 12/05/17 REPORTING LEVEL = 0.8 newdate = 12/04/17 REPORTING LEVEL = 0.8 newdate = 12/04/17 REPORTING LEVEL = 0.8 newdate = 11/21/17 REPORTING LEVEL = 0.8 newdate = 11/21/17 REPORTING LEVEL = 0.8 newdate = 09/28/17 REPORTING LEVEL = 0.8 newdate = 09/28/17 REPORTING LEVEL = 0.8 newdate = 08/30/17 REPORTING LEVEL = 0.8 newdate = 08/30/17 REPORTING LEVEL = 0.8 newdate = 08/30/17 REPORTING LEVEL = 0.8 newdate = 08/30/17 REPORTING LEVEL = 0.8 newdate = 07/26/17 REPORTING LEVEL = 0.8 newdate = 07/26/17 REPORTING LEVEL = 0.8 newdate = 07/26/17 REPORTING LEVEL = 0.8 newdate = 07/26/17 REPORTING LEVEL = 0.8 newdate = 06/30/17 REPORTING LEVEL = 0.8 newdate = 06/30/17 REPORTING LEVEL = 0.8 newdate = 06/30/17 REPORTING LEVEL = 0.8 newdate = 06/30/17 REPORTING LEVEL = 0.8 newdate = 03/15/17 REPORTING LEVEL = 0.8 newdate = 03/15/17 REPORTING LEVEL = 0.8 newdate = 03/15/17 REPORTING LEVEL = 0.8 newdate = 03/15/17 REPORTING LEVEL = 0.8 newdate = 02/24/17 REPORTING LEVEL = 0.8 newdate = 02/24/17 REPORTING LEVEL = 0.8 newdate = 02/01/17 REPORTING LEVEL = 0.8 newdate = 02/01/17 REPORTING LEVEL = 0.8 newdate = 12/29/16 REPORTING LEVEL = 0.8 newdate = 12/29/16 REPORTING LEVEL = 0.8 newdate = 12/15/16 REPORTING LEVEL = 0.8 newdate = 12/15/16 REPORTING LEVEL = 0.8 newdate = 12/07/16 REPORTING LEVEL = 0.8 newdate = 12/07/16 REPORTING LEVEL = 0.8 newdate = 09/21/16 REPORTING LEVEL = 0.8 newdate = 09/21/16 REPORTING LEVEL = 0.8 newdate = 09/15/16 REPORTING LEVEL = 0.8 newdate = 09/15/16 REPORTING LEVEL = 0.8 newdate = 09/09/16 REPORTING LEVEL = 0.8 newdate = 09/09/16 REPORTING LEVEL = 0.8 newdate = 08/31/16 REPORTING LEVEL = 0.8 newdate = 08/31/16 REPORTING LEVEL = 0.8 newdate = 08/19/16 REPORTING LEVEL = 0.8 newdate = 08/19/16 REPORTING LEVEL = 0.8 newdate = 08/11/16 REPORTING LEVEL = 0.8 newdate = 08/11/16 REPORTING LEVEL = 0.8 newdate = 07/12/16 REPORTING LEVEL = 0.8 newdate = 07/12/16 REPORTING LEVEL = 0.8 newdate = 06/24/16 REPORTING LEVEL = 0.8 newdate = 06/24/16 REPORTING LEVEL = 0.8 newdate = 03/18/16 REPORTING LEVEL = 0.8 newdate = 03/18/16 REPORTING LEVEL = 0.8 newdate = 03/18/16 REPORTING LEVEL = 0.8 newdate = 03/18/16 REPORTING LEVEL = 0.8 newdate = 03/07/16 REPORTING LEVEL = 0.8 newdate = 03/07/16 REPORTING LEVEL = 0.8 newdate = 03/07/16 REPORTING LEVEL = 0.8 Y = 0
The SGPlot Procedure

False Positive & Negative Listing for 17-ALPHA-ESTRADIOL

Status Lab ID Spike Mix Reporting Level Analysis Date Result Conc. Expected Conc.
False Negative 20160560045 Crescent 04EE007: 30 µl & Spex Organics EN150501025: 30 µl 0.8 03/18/16 < 0.8 1.2
  20161130024 Spex Organics EN150501025: 50 µl & ERA 0601-15-04: 50 µl 0.8 07/12/16 < 1.58 2
  20171790208 ChemService 5016100: 50 µl & Abs 052616: 50 µl 0.8 08/30/17 < 2.54 3.326316
False Positive 20161740282 Spex Organics TS160420010: 50 µl & ChemService 5016200: 50 µl 0.8 08/31/16 10.2 0

Updated 03/28/2018

back to table
Organic Blind Sample Program
False Positives & False Negatives
17-ALPHA-ETHYNYLESTRADIOL
Method: 4434 Testid: 64529GM005
Link to Individual Chart

newdate = 08/30/17 falseneg = -0.01 newdate = 07/26/17 falseneg = -0.01 newdate = 09/15/16 falseneg = -0.01 newdate = 09/09/16 falseneg = -0.01 newdate = 03/18/16 falseneg = -0.01 newdate = 03/18/16 falseneg = -0.01 newdate = 08/31/16 falsepos = 2.22 newdate = 03/07/16 falsepos = 0.42 newdate = 12/11/17 CENC_VAL = 8.130 newdate = 12/05/17 CENC_VAL = 7.400 newdate = 12/04/17 CENC_VAL = 1.000 newdate = 11/21/17 CENC_VAL = 1.150 newdate = 09/28/17 CENC_VAL = 2.730 newdate = 08/30/17 CENC_VAL = 2.790 newdate = 07/26/17 CENC_VAL = 4.180 newdate = 06/30/17 CENC_VAL = 5.090 newdate = 06/30/17 CENC_VAL = 3.420 newdate = 03/15/17 CENC_VAL = 3.970 newdate = 03/15/17 CENC_VAL = 1.940 newdate = 02/24/17 CENC_VAL = 2.710 newdate = 02/01/17 CENC_VAL = 1.740 newdate = 12/29/16 CENC_VAL = 1.560 newdate = 12/15/16 CENC_VAL = 2.840 newdate = 09/21/16 CENC_VAL = 2.840 newdate = 08/19/16 CENC_VAL = 3.020 newdate = 08/11/16 CENC_VAL = 2.770 newdate = 07/12/16 CENC_VAL = 1.720 newdate = 06/24/16 CENC_VAL = 1.060 newdate = 03/07/16 CENC_VAL = 2.070 newdate = 12/11/17 REPORTING LEVEL = 0.8 newdate = 12/05/17 REPORTING LEVEL = 0.8 newdate = 12/05/17 REPORTING LEVEL = 0.8 newdate = 12/04/17 REPORTING LEVEL = 0.8 newdate = 12/04/17 REPORTING LEVEL = 0.8 newdate = 11/21/17 REPORTING LEVEL = 0.8 newdate = 11/21/17 REPORTING LEVEL = 0.8 newdate = 09/28/17 REPORTING LEVEL = 0.8 newdate = 09/28/17 REPORTING LEVEL = 0.8 newdate = 08/30/17 REPORTING LEVEL = 0.8 newdate = 08/30/17 REPORTING LEVEL = 0.8 newdate = 08/30/17 REPORTING LEVEL = 0.8 newdate = 08/30/17 REPORTING LEVEL = 0.8 newdate = 07/26/17 REPORTING LEVEL = 0.8 newdate = 07/26/17 REPORTING LEVEL = 0.8 newdate = 07/26/17 REPORTING LEVEL = 0.8 newdate = 07/26/17 REPORTING LEVEL = 0.8 newdate = 06/30/17 REPORTING LEVEL = 0.8 newdate = 06/30/17 REPORTING LEVEL = 0.8 newdate = 06/30/17 REPORTING LEVEL = 0.8 newdate = 06/30/17 REPORTING LEVEL = 0.8 newdate = 03/15/17 REPORTING LEVEL = 0.8 newdate = 03/15/17 REPORTING LEVEL = 0.8 newdate = 03/15/17 REPORTING LEVEL = 0.8 newdate = 03/15/17 REPORTING LEVEL = 0.8 newdate = 02/24/17 REPORTING LEVEL = 0.8 newdate = 02/24/17 REPORTING LEVEL = 0.8 newdate = 02/01/17 REPORTING LEVEL = 0.8 newdate = 02/01/17 REPORTING LEVEL = 0.8 newdate = 12/29/16 REPORTING LEVEL = 0.8 newdate = 12/29/16 REPORTING LEVEL = 0.8 newdate = 12/15/16 REPORTING LEVEL = 0.8 newdate = 12/15/16 REPORTING LEVEL = 0.8 newdate = 12/07/16 REPORTING LEVEL = 0.8 newdate = 12/07/16 REPORTING LEVEL = 0.8 newdate = 09/21/16 REPORTING LEVEL = 0.8 newdate = 09/21/16 REPORTING LEVEL = 0.8 newdate = 09/15/16 REPORTING LEVEL = 0.8 newdate = 09/15/16 REPORTING LEVEL = 0.8 newdate = 09/09/16 REPORTING LEVEL = 0.8 newdate = 09/09/16 REPORTING LEVEL = 0.8 newdate = 08/31/16 REPORTING LEVEL = 0.8 newdate = 08/31/16 REPORTING LEVEL = 0.8 newdate = 08/19/16 REPORTING LEVEL = 0.8 newdate = 08/19/16 REPORTING LEVEL = 0.8 newdate = 08/11/16 REPORTING LEVEL = 0.8 newdate = 08/11/16 REPORTING LEVEL = 0.8 newdate = 07/12/16 REPORTING LEVEL = 0.8 newdate = 07/12/16 REPORTING LEVEL = 0.8 newdate = 06/24/16 REPORTING LEVEL = 0.8 newdate = 06/24/16 REPORTING LEVEL = 0.8 newdate = 03/18/16 REPORTING LEVEL = 0.8 newdate = 03/18/16 REPORTING LEVEL = 0.8 newdate = 03/18/16 REPORTING LEVEL = 0.8 newdate = 03/18/16 REPORTING LEVEL = 0.8 newdate = 03/07/16 REPORTING LEVEL = 0.8 newdate = 03/07/16 REPORTING LEVEL = 0.8 newdate = 03/07/16 REPORTING LEVEL = 0.8 Y = 0
The SGPlot Procedure

False Positive & Negative Listing for 17-ALPHA-ETHYNYLESTRADIOL

Status Lab ID Spike Mix Reporting Level Analysis Date Result Conc. Expected Conc.
False Negative 20160430110 Supelco LC13547: 30 µl & ChemService 4073900: 30 µl 0.8 03/18/16 < 0.8 1.2
  20160630047 Spex Organics EN150501025: 30 µl & Supelco LC13547: 30 µl 0.8 03/18/16 < 0.8 1.2
  20161820010 ChemService 5016200: 30 µl & Supelco LC20140V: 30 µl 0.8 09/09/16 < 1.84 2.021053
  20161960002 Supelco LC20140V: 30 µl & Spex Organics EN160621015: 30 µl 0.8 09/15/16 < 0.8 2.021053
  20171510081 Supelco LC20140V: 30 µl & ChemService 5016200: 30 µl 0.8 07/26/17 < 0.8 2.021053
  20171790208 ChemService 5016100: 50 µl & Abs 052616: 50 µl 0.8 08/30/17 < 2 3.368421
False Positive 20160070058 ChemService 4073900: 30 µl & Abs 041515: 30 µl 0.8 03/07/16 0.42 0
  20161740282 Spex Organics TS160420010: 50 µl & ChemService 5016200: 50 µl 0.8 08/31/16 2.22 0

Updated 03/28/2018

back to table
Organic Blind Sample Program
False Positives & False Negatives
17-BETA-ESTRADIOL
Method: 4434 Testid: 64530GM005
Link to Individual Chart

newdate = 08/30/17 falseneg = -0.01 newdate = 08/30/17 falseneg = -0.01 newdate = 07/25/17 falseneg = -0.01 newdate = 06/02/17 falseneg = -0.01 newdate = 06/02/17 falseneg = -0.01 newdate = 12/05/16 falseneg = -0.01 newdate = 07/12/16 falseneg = -0.01 newdate = 03/18/16 falseneg = -0.01 newdate = 03/18/16 falseneg = -0.01 newdate = 12/11/17 falsepos = 0.9 newdate = 12/11/17 CENC_VAL = 18.700 newdate = 12/05/17 CENC_VAL = 13.800 newdate = 12/04/17 CENC_VAL = 2.200 newdate = 11/21/17 CENC_VAL = 2.100 newdate = 09/05/17 CENC_VAL = 2.400 newdate = 07/28/17 CENC_VAL = 2.100 newdate = 07/26/17 CENC_VAL = 4.100 newdate = 07/25/17 CENC_VAL = 1.700 newdate = 07/13/17 CENC_VAL = 2.800 newdate = 03/15/17 CENC_VAL = 4.200 newdate = 02/01/17 CENC_VAL = 1.900 newdate = 01/13/17 CENC_VAL = 1.900 newdate = 12/29/16 CENC_VAL = 1.800 newdate = 09/16/16 CENC_VAL = 1.600 newdate = 09/15/16 CENC_VAL = 1.200 newdate = 08/31/16 CENC_VAL = 2456.000 newdate = 08/19/16 CENC_VAL = 2547.000 newdate = 08/11/16 CENC_VAL = 1811.000 newdate = 06/24/16 CENC_VAL = 1.700 newdate = 03/07/16 CENC_VAL = 1.700 newdate = 03/07/16 CENC_VAL = 1.190 newdate = 12/11/17 REPORTING LEVEL = 1.6 newdate = 12/11/17 REPORTING LEVEL = 1.6 newdate = 12/11/17 REPORTING LEVEL = 1.6 newdate = 12/05/17 REPORTING LEVEL = 1.6 newdate = 12/05/17 REPORTING LEVEL = 1.6 newdate = 12/04/17 REPORTING LEVEL = 1.6 newdate = 12/04/17 REPORTING LEVEL = 1.6 newdate = 11/21/17 REPORTING LEVEL = 1.6 newdate = 11/21/17 REPORTING LEVEL = 1.6 newdate = 09/05/17 REPORTING LEVEL = 1.6 newdate = 09/05/17 REPORTING LEVEL = 1.6 newdate = 08/30/17 REPORTING LEVEL = 1.6 newdate = 08/30/17 REPORTING LEVEL = 1.6 newdate = 08/30/17 REPORTING LEVEL = 1.6 newdate = 08/30/17 REPORTING LEVEL = 1.6 newdate = 07/28/17 REPORTING LEVEL = 1.6 newdate = 07/28/17 REPORTING LEVEL = 1.6 newdate = 07/26/17 REPORTING LEVEL = 1.6 newdate = 07/26/17 REPORTING LEVEL = 1.6 newdate = 07/25/17 REPORTING LEVEL = 1.6 newdate = 07/25/17 REPORTING LEVEL = 1.6 newdate = 07/25/17 REPORTING LEVEL = 1.6 newdate = 07/25/17 REPORTING LEVEL = 1.6 newdate = 07/13/17 REPORTING LEVEL = 1.6 newdate = 07/13/17 REPORTING LEVEL = 1.6 newdate = 06/02/17 REPORTING LEVEL = 1.6 newdate = 06/02/17 REPORTING LEVEL = 1.6 newdate = 06/02/17 REPORTING LEVEL = 1.6 newdate = 06/02/17 REPORTING LEVEL = 1.6 newdate = 03/15/17 REPORTING LEVEL = 1.6 newdate = 03/15/17 REPORTING LEVEL = 1.6 newdate = 02/01/17 REPORTING LEVEL = 1.6 newdate = 02/01/17 REPORTING LEVEL = 1.6 newdate = 01/13/17 REPORTING LEVEL = 1.6 newdate = 01/13/17 REPORTING LEVEL = 1.6 newdate = 12/29/16 REPORTING LEVEL = 1.6 newdate = 12/29/16 REPORTING LEVEL = 1.6 newdate = 12/07/16 REPORTING LEVEL = 1.6 newdate = 12/07/16 REPORTING LEVEL = 1.6 newdate = 12/05/16 REPORTING LEVEL = 1.6 newdate = 12/05/16 REPORTING LEVEL = 1.6 newdate = 09/16/16 REPORTING LEVEL = 1.6 newdate = 09/16/16 REPORTING LEVEL = 1.6 newdate = 09/15/16 REPORTING LEVEL = 1.6 newdate = 09/15/16 REPORTING LEVEL = 1.6 newdate = 08/31/16 REPORTING LEVEL = 1.6 newdate = 08/31/16 REPORTING LEVEL = 1.6 newdate = 08/19/16 REPORTING LEVEL = 1.6 newdate = 08/19/16 REPORTING LEVEL = 1.6 newdate = 08/11/16 REPORTING LEVEL = 1.6 newdate = 08/11/16 REPORTING LEVEL = 1.6 newdate = 07/12/16 REPORTING LEVEL = 1.6 newdate = 07/12/16 REPORTING LEVEL = 1.6 newdate = 06/24/16 REPORTING LEVEL = 1.6 newdate = 06/24/16 REPORTING LEVEL = 1.6 newdate = 03/18/16 REPORTING LEVEL = 0.8 newdate = 03/18/16 REPORTING LEVEL = 0.8 newdate = 03/18/16 REPORTING LEVEL = 0.8 newdate = 03/18/16 REPORTING LEVEL = 0.8 newdate = 03/07/16 REPORTING LEVEL = 0.8 newdate = 03/07/16 REPORTING LEVEL = 0.8 newdate = 03/07/16 REPORTING LEVEL = 0.8 Y = 0
The SGPlot Procedure

False Positive & Negative Listing for 17-BETA-ESTRADIOL

Status Lab ID Spike Mix Reporting Level Analysis Date Result Conc. Expected Conc.
False Negative 20160560045 Crescent 04EE007: 30 µl & Spex Organics EN150501025: 30 µl 0.8 03/18/16 < 0.92 1.2
  20160630047 Spex Organics EN150501025: 30 µl & Supelco LC13547: 30 µl 0.8 03/18/16 < 0.8 1.2
  20161130024 Spex Organics EN150501025: 50 µl & ERA 0601-15-04: 50 µl 1.6 07/12/16 < 1.9 2
  20162300273 Abs 052616: 30 µl & Abs 061416H: 30 µl 1.6 12/05/16 < 1.7 2.027368
  20170320040 Abs 052616: 50 µl & Abs 061416H: 50 µl 1.6 06/02/17 < 2.9 3.378947
  20170320041 Abs 052616: 50 µl & Abs 061416H: 50 µl 1.6 06/02/17 < 1.6 3.378947
  20171230084 Spex Organics EN160621015: 30 µl & Abs 061416H: 30 µl 1.6 07/25/17 < 1.6 1.976842
  20171720141 Supelco LC20140V: 80 µl & Spex Organics EN160621015: 80 µl 1.6 08/30/17 < 4.1 5.271579
  20171790208 ChemService 5016100: 50 µl & Abs 052616: 50 µl 1.6 08/30/17 < 2.9 3.378947
False Positive 20172430120 Spex Organics CT170727012: 50 µl & Spex Organics EN170728012: 50 µl 1.6 12/11/17 0.9 0

Updated 03/28/2018

back to table
Organic Blind Sample Program
False Positives & False Negatives
3-BETA-COPROSTANOL
Method: 4434 Testid: 64532GM005
Link to Individual Chart

newdate = 11/21/17 falseneg = -0.01 newdate = 02/01/17 falseneg = -0.01 newdate = 12/29/16 falseneg = -0.01 newdate = 09/21/16 falseneg = -0.01 newdate = 03/18/16 falseneg = -0.01 newdate = 03/18/16 falseneg = -0.01 newdate = 03/07/16 falseneg = -0.01 newdate = 12/11/17 CENC_VAL = 2326.000 newdate = 12/05/17 CENC_VAL = 1800.000 newdate = 12/04/17 CENC_VAL = 242.000 newdate = 09/28/17 CENC_VAL = 456.000 newdate = 08/30/17 CENC_VAL = 1033.000 newdate = 08/30/17 CENC_VAL = 599.000 newdate = 07/26/17 CENC_VAL = 663.000 newdate = 07/26/17 CENC_VAL = 249.000 newdate = 06/30/17 CENC_VAL = 439.000 newdate = 06/30/17 CENC_VAL = 869.000 newdate = 03/15/17 CENC_VAL = 825.000 newdate = 03/15/17 CENC_VAL = 260.000 newdate = 02/24/17 CENC_VAL = 413.000 newdate = 12/15/16 CENC_VAL = 383.000 newdate = 09/15/16 CENC_VAL = 223.000 newdate = 09/09/16 CENC_VAL = 226.000 newdate = 08/19/16 CENC_VAL = 360.000 newdate = 08/11/16 CENC_VAL = 464.000 newdate = 07/12/16 CENC_VAL = 370.000 newdate = 06/24/16 CENC_VAL = 272.000 newdate = 03/07/16 CENC_VAL = 280.000 newdate = 12/11/17 REPORTING LEVEL = 200 newdate = 12/05/17 REPORTING LEVEL = 200 newdate = 12/05/17 REPORTING LEVEL = 200 newdate = 12/04/17 REPORTING LEVEL = 200 newdate = 12/04/17 REPORTING LEVEL = 200 newdate = 11/21/17 REPORTING LEVEL = 200 newdate = 11/21/17 REPORTING LEVEL = 200 newdate = 09/28/17 REPORTING LEVEL = 200 newdate = 09/28/17 REPORTING LEVEL = 200 newdate = 08/30/17 REPORTING LEVEL = 200 newdate = 08/30/17 REPORTING LEVEL = 200 newdate = 08/30/17 REPORTING LEVEL = 200 newdate = 08/30/17 REPORTING LEVEL = 200 newdate = 07/26/17 REPORTING LEVEL = 200 newdate = 07/26/17 REPORTING LEVEL = 200 newdate = 07/26/17 REPORTING LEVEL = 200 newdate = 07/26/17 REPORTING LEVEL = 200 newdate = 06/30/17 REPORTING LEVEL = 200 newdate = 06/30/17 REPORTING LEVEL = 200 newdate = 06/30/17 REPORTING LEVEL = 200 newdate = 06/30/17 REPORTING LEVEL = 200 newdate = 03/15/17 REPORTING LEVEL = 200 newdate = 03/15/17 REPORTING LEVEL = 200 newdate = 03/15/17 REPORTING LEVEL = 200 newdate = 03/15/17 REPORTING LEVEL = 200 newdate = 02/24/17 REPORTING LEVEL = 200 newdate = 02/24/17 REPORTING LEVEL = 200 newdate = 02/01/17 REPORTING LEVEL = 200 newdate = 02/01/17 REPORTING LEVEL = 200 newdate = 12/29/16 REPORTING LEVEL = 200 newdate = 12/29/16 REPORTING LEVEL = 200 newdate = 12/15/16 REPORTING LEVEL = 200 newdate = 12/15/16 REPORTING LEVEL = 200 newdate = 12/07/16 REPORTING LEVEL = 200 newdate = 12/07/16 REPORTING LEVEL = 200 newdate = 09/21/16 REPORTING LEVEL = 200 newdate = 09/21/16 REPORTING LEVEL = 200 newdate = 09/15/16 REPORTING LEVEL = 200 newdate = 09/15/16 REPORTING LEVEL = 200 newdate = 09/09/16 REPORTING LEVEL = 200 newdate = 09/09/16 REPORTING LEVEL = 200 newdate = 08/19/16 REPORTING LEVEL = 200 newdate = 08/19/16 REPORTING LEVEL = 200 newdate = 08/11/16 REPORTING LEVEL = 200 newdate = 08/11/16 REPORTING LEVEL = 200 newdate = 07/12/16 REPORTING LEVEL = 200 newdate = 07/12/16 REPORTING LEVEL = 200 newdate = 06/24/16 REPORTING LEVEL = 200 newdate = 06/24/16 REPORTING LEVEL = 200 newdate = 03/18/16 REPORTING LEVEL = 200 newdate = 03/18/16 REPORTING LEVEL = 200 newdate = 03/18/16 REPORTING LEVEL = 200 newdate = 03/18/16 REPORTING LEVEL = 200 newdate = 03/07/16 REPORTING LEVEL = 200 newdate = 03/07/16 REPORTING LEVEL = 200 newdate = 03/07/16 REPORTING LEVEL = 200 Y = 0
The SGPlot Procedure

False Positive & Negative Listing for 3-BETA-COPROSTANOL

Status Lab ID Spike Mix Reporting Level Analysis Date Result Conc. Expected Conc.
False Negative 20160070058 ChemService 4073900: 30 µl & Abs 041515: 30 µl 200 03/07/16 < 200 297.2564
  20160560045 Crescent 04EE007: 30 µl & Spex Organics EN150501025: 30 µl 200 03/18/16 < 200 300
  20160630047 Spex Organics EN150501025: 30 µl & Supelco LC13547: 30 µl 200 03/18/16 < 200 300
  20162100009 ChemService 5016200: 30 µl & ChemService 5016100: 30 µl 200 09/21/16 < 230 500.2105
  20162800003 ChemService 5016100: 30 µl & Abs 052616: 30 µl 200 12/29/16 < 227 500.2105
  20163220167 Supelco LC20140V: 30 µl & Abs 052616: 30 µl 200 02/01/17 < 245 500.2105
  20172230002 ChemService 6460700: 10 µl & ChemService 6494400: 10 µl 200 11/21/17 < 200 402

Updated 03/28/2018

back to table
Organic Blind Sample Program
False Positives & False Negatives
4,4BISPHENOL_F
Method: 4434 Testid: 51294GM005
Link to Individual Chart

newdate = 09/05/17 CENC_VAL = 21.000 newdate = 07/28/17 CENC_VAL = 26.000 newdate = 07/25/17 CENC_VAL = 25.000 newdate = 07/25/17 CENC_VAL = 17.000 newdate = 06/30/17 CENC_VAL = 47.000 newdate = 06/30/17 CENC_VAL = 38.000 newdate = 06/02/17 CENC_VAL = 19.000 newdate = 06/02/17 CENC_VAL = 22.000 newdate = 02/24/17 CENC_VAL = 28.000 newdate = 12/15/16 CENC_VAL = 34.000 newdate = 12/05/16 CENC_VAL = 23.000 newdate = 07/12/16 CENC_VAL = 16.000 newdate = 06/24/16 CENC_VAL = 40.000 newdate = 03/18/16 CENC_VAL = 12.000 newdate = 03/18/16 CENC_VAL = 13.000 newdate = 03/07/16 CENC_VAL = 29.000 newdate = 03/07/16 CENC_VAL = 18.000 newdate = 09/05/17 REPORTING LEVEL = 10 newdate = 07/28/17 REPORTING LEVEL = 10 newdate = 07/28/17 REPORTING LEVEL = 10 newdate = 07/25/17 REPORTING LEVEL = 10 newdate = 07/25/17 REPORTING LEVEL = 10 newdate = 07/25/17 REPORTING LEVEL = 10 newdate = 07/25/17 REPORTING LEVEL = 10 newdate = 06/30/17 REPORTING LEVEL = 10 newdate = 06/30/17 REPORTING LEVEL = 10 newdate = 06/30/17 REPORTING LEVEL = 10 newdate = 06/30/17 REPORTING LEVEL = 10 newdate = 06/02/17 REPORTING LEVEL = 10 newdate = 06/02/17 REPORTING LEVEL = 10 newdate = 06/02/17 REPORTING LEVEL = 10 newdate = 06/02/17 REPORTING LEVEL = 10 newdate = 02/24/17 REPORTING LEVEL = 10 newdate = 02/24/17 REPORTING LEVEL = 10 newdate = 12/15/16 REPORTING LEVEL = 10 newdate = 12/15/16 REPORTING LEVEL = 10 newdate = 12/07/16 REPORTING LEVEL = 10 newdate = 12/07/16 REPORTING LEVEL = 10 newdate = 12/05/16 REPORTING LEVEL = 10 newdate = 12/05/16 REPORTING LEVEL = 10 newdate = 07/12/16 REPORTING LEVEL = 10 newdate = 07/12/16 REPORTING LEVEL = 10 newdate = 06/24/16 REPORTING LEVEL = 10 newdate = 06/24/16 REPORTING LEVEL = 10 newdate = 03/18/16 REPORTING LEVEL = 10 newdate = 03/18/16 REPORTING LEVEL = 10 newdate = 03/18/16 REPORTING LEVEL = 10 newdate = 03/18/16 REPORTING LEVEL = 10 newdate = 03/07/16 REPORTING LEVEL = 10 newdate = 03/07/16 REPORTING LEVEL = 10 newdate = 03/07/16 REPORTING LEVEL = 10
The SGPlot Procedure

back to table
Organic Blind Sample Program
False Positives & False Negatives
4-ANDROSTENE-3,17-DIONE
Method: 4434 Testid: 64533GM005
Link to Individual Chart

newdate = 09/05/17 falseneg = -0.01 newdate = 06/30/17 falseneg = -0.01 newdate = 12/15/16 falseneg = -0.01 newdate = 12/05/16 falseneg = -0.01 newdate = 08/19/16 falsepos = 7.9 newdate = 12/11/17 CENC_VAL = 4.900 newdate = 07/28/17 CENC_VAL = 20.000 newdate = 07/25/17 CENC_VAL = 5.400 newdate = 07/25/17 CENC_VAL = 7.900 newdate = 06/30/17 CENC_VAL = 9.000 newdate = 06/02/17 CENC_VAL = 20.000 newdate = 06/02/17 CENC_VAL = 20.000 newdate = 02/24/17 CENC_VAL = 1.200 newdate = 06/24/16 CENC_VAL = 3.300 newdate = 03/18/16 CENC_VAL = 20.000 newdate = 12/11/17 REPORTING LEVEL = 2 newdate = 09/05/17 REPORTING LEVEL = 2 newdate = 09/05/17 REPORTING LEVEL = 2 newdate = 07/28/17 REPORTING LEVEL = 2 newdate = 07/28/17 REPORTING LEVEL = 2 newdate = 07/25/17 REPORTING LEVEL = 2 newdate = 07/25/17 REPORTING LEVEL = 2 newdate = 07/25/17 REPORTING LEVEL = 2 newdate = 07/25/17 REPORTING LEVEL = 2 newdate = 06/30/17 REPORTING LEVEL = 2 newdate = 06/30/17 REPORTING LEVEL = 2 newdate = 06/30/17 REPORTING LEVEL = 2 newdate = 06/30/17 REPORTING LEVEL = 2 newdate = 06/02/17 REPORTING LEVEL = 2 newdate = 06/02/17 REPORTING LEVEL = 2 newdate = 06/02/17 REPORTING LEVEL = 2 newdate = 06/02/17 REPORTING LEVEL = 2 newdate = 02/24/17 REPORTING LEVEL = 2 newdate = 02/24/17 REPORTING LEVEL = 2 newdate = 12/15/16 REPORTING LEVEL = 2 newdate = 12/15/16 REPORTING LEVEL = 2 newdate = 12/07/16 REPORTING LEVEL = 2 newdate = 12/07/16 REPORTING LEVEL = 2 newdate = 12/05/16 REPORTING LEVEL = 2 newdate = 12/05/16 REPORTING LEVEL = 2 newdate = 08/19/16 REPORTING LEVEL = 2 newdate = 08/19/16 REPORTING LEVEL = 2 newdate = 06/24/16 REPORTING LEVEL = 2 newdate = 06/24/16 REPORTING LEVEL = 2 newdate = 03/18/16 REPORTING LEVEL = 0.8 Y = 0
The SGPlot Procedure

False Positive & Negative Listing for 4-ANDROSTENE-3,17-DIONE

Status Lab ID Spike Mix Reporting Level Analysis Date Result Conc. Expected Conc.
False Negative 20162300273 Abs 052616: 30 µl & Abs 061416H: 30 µl 2 12/05/16 < 2 2.029895
  20162520002 Abs 061416H: 50 µl & ChemService 5016100: 50 µl 2 12/15/16 < 2 3.383158
  20170740061 Abs 061416H: 80 µl & ChemService 5016100: 80 µl 2 06/30/17 < 4 5.413053
  20172020154 Spex Organics EN160621015: 50 µl & Abs 061416H: 50 µl 2 09/05/17 < 2 3.383158
False Positive 20161540125 Supelco LC20140V: 50 µl & Spex Organics TS160420010: 50 µl 2 08/19/16 E 7.9 0

Updated 03/28/2018

back to table
Organic Blind Sample Program
False Positives & False Negatives
BISPHENOL_A
Method: 4434 Testid: 67305GM005
Link to Individual Chart

newdate = 12/13/17 CENC_VAL = 1147.000 newdate = 12/13/17 CENC_VAL = 116.000 newdate = 12/11/17 CENC_VAL = 619.000 newdate = 09/28/17 CENC_VAL = 296.000 newdate = 09/05/17 CENC_VAL = 206.000 newdate = 07/28/17 CENC_VAL = 233.000 newdate = 07/26/17 CENC_VAL = 144.000 newdate = 07/25/17 CENC_VAL = 221.000 newdate = 07/25/17 CENC_VAL = 144.000 newdate = 07/13/17 CENC_VAL = 238.000 newdate = 06/30/17 CENC_VAL = 460.000 newdate = 06/30/17 CENC_VAL = 387.000 newdate = 06/02/17 CENC_VAL = 188.000 newdate = 06/02/17 CENC_VAL = 216.000 newdate = 03/15/17 CENC_VAL = 169.000 newdate = 02/24/17 CENC_VAL = 256.000 newdate = 01/13/17 CENC_VAL = 164.000 newdate = 12/15/16 CENC_VAL = 307.000 newdate = 12/05/16 CENC_VAL = 173.000 newdate = 09/21/16 CENC_VAL = 239.000 newdate = 09/16/16 CENC_VAL = 182.000 newdate = 09/09/16 CENC_VAL = 176.000 newdate = 08/31/16 CENC_VAL = 323.000 newdate = 07/12/16 CENC_VAL = 138.000 newdate = 06/24/16 CENC_VAL = 336.000 newdate = 03/18/16 CENC_VAL = 120.000 newdate = 03/18/16 CENC_VAL = 120.000 newdate = 03/07/16 CENC_VAL = 100.000 newdate = 12/13/17 REPORTING LEVEL = 100 newdate = 12/13/17 REPORTING LEVEL = 100 newdate = 12/13/17 REPORTING LEVEL = 100 newdate = 12/11/17 REPORTING LEVEL = 100 newdate = 12/11/17 REPORTING LEVEL = 100 newdate = 09/28/17 REPORTING LEVEL = 100 newdate = 09/28/17 REPORTING LEVEL = 100 newdate = 09/05/17 REPORTING LEVEL = 100 newdate = 09/05/17 REPORTING LEVEL = 100 newdate = 07/28/17 REPORTING LEVEL = 100 newdate = 07/28/17 REPORTING LEVEL = 100 newdate = 07/26/17 REPORTING LEVEL = 100 newdate = 07/26/17 REPORTING LEVEL = 100 newdate = 07/25/17 REPORTING LEVEL = 100 newdate = 07/25/17 REPORTING LEVEL = 100 newdate = 07/25/17 REPORTING LEVEL = 100 newdate = 07/25/17 REPORTING LEVEL = 100 newdate = 07/13/17 REPORTING LEVEL = 100 newdate = 07/13/17 REPORTING LEVEL = 100 newdate = 06/30/17 REPORTING LEVEL = 100 newdate = 06/30/17 REPORTING LEVEL = 100 newdate = 06/30/17 REPORTING LEVEL = 100 newdate = 06/30/17 REPORTING LEVEL = 100 newdate = 06/02/17 REPORTING LEVEL = 100 newdate = 06/02/17 REPORTING LEVEL = 100 newdate = 06/02/17 REPORTING LEVEL = 100 newdate = 06/02/17 REPORTING LEVEL = 100 newdate = 03/15/17 REPORTING LEVEL = 100 newdate = 03/15/17 REPORTING LEVEL = 100 newdate = 02/24/17 REPORTING LEVEL = 100 newdate = 02/24/17 REPORTING LEVEL = 100 newdate = 01/13/17 REPORTING LEVEL = 100 newdate = 01/13/17 REPORTING LEVEL = 100 newdate = 12/15/16 REPORTING LEVEL = 100 newdate = 12/15/16 REPORTING LEVEL = 100 newdate = 12/07/16 REPORTING LEVEL = 100 newdate = 12/07/16 REPORTING LEVEL = 100 newdate = 12/05/16 REPORTING LEVEL = 100 newdate = 12/05/16 REPORTING LEVEL = 100 newdate = 09/21/16 REPORTING LEVEL = 100 newdate = 09/21/16 REPORTING LEVEL = 100 newdate = 09/16/16 REPORTING LEVEL = 100 newdate = 09/16/16 REPORTING LEVEL = 100 newdate = 09/09/16 REPORTING LEVEL = 100 newdate = 09/09/16 REPORTING LEVEL = 100 newdate = 08/31/16 REPORTING LEVEL = 100 newdate = 08/31/16 REPORTING LEVEL = 100 newdate = 07/12/16 REPORTING LEVEL = 100 newdate = 07/12/16 REPORTING LEVEL = 100 newdate = 06/24/16 REPORTING LEVEL = 100 newdate = 06/24/16 REPORTING LEVEL = 100 newdate = 03/18/16 REPORTING LEVEL = 100 newdate = 03/18/16 REPORTING LEVEL = 100 newdate = 03/18/16 REPORTING LEVEL = 100 newdate = 03/18/16 REPORTING LEVEL = 100 newdate = 03/07/16 REPORTING LEVEL = 100
The SGPlot Procedure

back to table
Organic Blind Sample Program
False Positives & False Negatives
CHOLESTEROL
Method: 4434 Testid: 64534GM005
Link to Individual Chart

newdate = 07/26/17 falseneg = -0.01 newdate = 07/25/17 falseneg = -0.01 newdate = 03/15/17 falseneg = -0.01 newdate = 02/24/17 falseneg = -0.01 newdate = 01/13/17 falseneg = -0.01 newdate = 12/05/16 falseneg = -0.01 newdate = 09/21/16 falseneg = -0.01 newdate = 09/16/16 falseneg = -0.01 newdate = 09/09/16 falseneg = -0.01 newdate = 06/24/16 falseneg = -0.01 newdate = 06/24/16 falseneg = -0.01 newdate = 03/18/16 falseneg = -0.01 newdate = 03/07/16 falseneg = -0.01 newdate = 12/13/17 CENC_VAL = 5446.000 newdate = 12/13/17 CENC_VAL = 575.000 newdate = 12/11/17 CENC_VAL = 3280.000 newdate = 09/28/17 CENC_VAL = 628.000 newdate = 09/05/17 CENC_VAL = 468.000 newdate = 07/28/17 CENC_VAL = 505.000 newdate = 07/25/17 CENC_VAL = 517.000 newdate = 07/13/17 CENC_VAL = 452.000 newdate = 06/30/17 CENC_VAL = 1063.000 newdate = 06/30/17 CENC_VAL = 994.000 newdate = 06/02/17 CENC_VAL = 447.000 newdate = 06/02/17 CENC_VAL = 542.000 newdate = 12/15/16 CENC_VAL = 510.000 newdate = 08/31/16 CENC_VAL = 601.000 newdate = 03/18/16 CENC_VAL = 209.000 newdate = 12/13/17 REPORTING LEVEL = 400 newdate = 12/13/17 REPORTING LEVEL = 400 newdate = 12/13/17 REPORTING LEVEL = 400 newdate = 12/11/17 REPORTING LEVEL = 400 newdate = 12/11/17 REPORTING LEVEL = 400 newdate = 09/28/17 REPORTING LEVEL = 400 newdate = 09/28/17 REPORTING LEVEL = 400 newdate = 09/05/17 REPORTING LEVEL = 400 newdate = 09/05/17 REPORTING LEVEL = 400 newdate = 07/28/17 REPORTING LEVEL = 400 newdate = 07/28/17 REPORTING LEVEL = 400 newdate = 07/26/17 REPORTING LEVEL = 400 newdate = 07/26/17 REPORTING LEVEL = 400 newdate = 07/25/17 REPORTING LEVEL = 400 newdate = 07/25/17 REPORTING LEVEL = 400 newdate = 07/25/17 REPORTING LEVEL = 400 newdate = 07/25/17 REPORTING LEVEL = 400 newdate = 07/13/17 REPORTING LEVEL = 400 newdate = 07/13/17 REPORTING LEVEL = 400 newdate = 06/30/17 REPORTING LEVEL = 400 newdate = 06/30/17 REPORTING LEVEL = 400 newdate = 06/30/17 REPORTING LEVEL = 400 newdate = 06/30/17 REPORTING LEVEL = 400 newdate = 06/02/17 REPORTING LEVEL = 400 newdate = 06/02/17 REPORTING LEVEL = 400 newdate = 06/02/17 REPORTING LEVEL = 400 newdate = 06/02/17 REPORTING LEVEL = 400 newdate = 03/15/17 REPORTING LEVEL = 400 newdate = 03/15/17 REPORTING LEVEL = 400 newdate = 02/24/17 REPORTING LEVEL = 400 newdate = 02/24/17 REPORTING LEVEL = 400 newdate = 01/13/17 REPORTING LEVEL = 400 newdate = 01/13/17 REPORTING LEVEL = 400 newdate = 12/15/16 REPORTING LEVEL = 400 newdate = 12/15/16 REPORTING LEVEL = 400 newdate = 12/07/16 REPORTING LEVEL = 400 newdate = 12/07/16 REPORTING LEVEL = 400 newdate = 12/05/16 REPORTING LEVEL = 400 newdate = 12/05/16 REPORTING LEVEL = 400 newdate = 09/21/16 REPORTING LEVEL = 400 newdate = 09/21/16 REPORTING LEVEL = 400 newdate = 09/16/16 REPORTING LEVEL = 400 newdate = 09/16/16 REPORTING LEVEL = 400 newdate = 09/09/16 REPORTING LEVEL = 400 newdate = 09/09/16 REPORTING LEVEL = 400 newdate = 08/31/16 REPORTING LEVEL = 400 newdate = 08/31/16 REPORTING LEVEL = 400 newdate = 06/24/16 REPORTING LEVEL = 400 newdate = 06/24/16 REPORTING LEVEL = 400 newdate = 06/24/16 REPORTING LEVEL = 400 newdate = 06/24/16 REPORTING LEVEL = 400 newdate = 03/18/16 REPORTING LEVEL = 200 newdate = 03/18/16 REPORTING LEVEL = 200 newdate = 03/18/16 REPORTING LEVEL = 200 newdate = 03/18/16 REPORTING LEVEL = 200 newdate = 03/07/16 REPORTING LEVEL = 200 Y = 0
The SGPlot Procedure

False Positive & Negative Listing for CHOLESTEROL

Status Lab ID Spike Mix Reporting Level Analysis Date Result Conc. Expected Conc.
False Negative 20160070058 ChemService 4073900: 30 µl & Abs 041515: 30 µl 200 03/07/16 < 200 299.9431
  20160560045 Crescent 04EE007: 30 µl & Spex Organics EN150501025: 30 µl 200 03/18/16 < 200 298.4842
  20160840085 ERA 0601-15-04: 50 µl & ChemService 4073900: 50 µl 400 06/24/16 < 400 499.9053
  20160910145 Crescent 04EE007: 50 µl & Spex Organics EN150501025: 50 µl 400 06/24/16 < 400 497.4737
  20161820010 ChemService 5016200: 30 µl & Supelco LC20140V: 30 µl 400 09/09/16 < 400 500.5389
  20162020125 Spex Organics EN160621015: 30 µl & ChemService 5016200: 30 µl 400 09/16/16 < 400 500.5389
  20162100009 ChemService 5016200: 30 µl & ChemService 5016100: 30 µl 400 09/21/16 < 400 500.5389
  20162300273 Abs 052616: 30 µl & Abs 061416H: 30 µl 400 12/05/16 < 400 500.3855
  20162930166 Abs 052616: 30 µl & ChemService 5016200: 30 µl 400 01/13/17 < 421 500.5389
  20163070095 Abs 061416H: 50 µl & Supelco LC20140V: 50 µl 400 02/24/17 < 592 833.9758
  20163630037 ChemService 5016200: 30 µl & Supelco LC20140V: 30 µl 400 03/15/17 < 400 500.5389
  20171230084 Spex Organics EN160621015: 30 µl & Abs 061416H: 30 µl 400 07/25/17 < 400 500.3855
  20171510081 Supelco LC20140V: 30 µl & ChemService 5016200: 30 µl 400 07/26/17 < 400 500.5389

Updated 03/28/2018

back to table
Organic Blind Sample Program
False Positives & False Negatives
CIS-ANDROSTERONE
Method: 4434 Testid: 64535GM005
Link to Individual Chart

newdate = 09/21/16 falseneg = -0.01 newdate = 07/12/16 falseneg = -0.01 newdate = 06/24/16 falseneg = -0.01 newdate = 12/13/17 CENC_VAL = 17.800 newdate = 12/13/17 CENC_VAL = 2.300 newdate = 12/11/17 CENC_VAL = 16.200 newdate = 12/11/17 CENC_VAL = 11.600 newdate = 12/05/17 CENC_VAL = 13.300 newdate = 12/04/17 CENC_VAL = 1.700 newdate = 11/21/17 CENC_VAL = 2.200 newdate = 09/28/17 CENC_VAL = 1.900 newdate = 08/30/17 CENC_VAL = 2.900 newdate = 08/30/17 CENC_VAL = 1.400 newdate = 07/26/17 CENC_VAL = 3.500 newdate = 07/26/17 CENC_VAL = 1.200 newdate = 06/30/17 CENC_VAL = 4.700 newdate = 06/30/17 CENC_VAL = 2.700 newdate = 03/15/17 CENC_VAL = 3.200 newdate = 03/15/17 CENC_VAL = 1.100 newdate = 02/24/17 CENC_VAL = 3.200 newdate = 02/01/17 CENC_VAL = 1.400 newdate = 12/29/16 CENC_VAL = 2.200 newdate = 12/15/16 CENC_VAL = 2.600 newdate = 09/15/16 CENC_VAL = 2.000 newdate = 09/09/16 CENC_VAL = 2.000 newdate = 08/19/16 CENC_VAL = 2.800 newdate = 08/11/16 CENC_VAL = 3.300 newdate = 03/18/16 CENC_VAL = 20.000 newdate = 03/18/16 CENC_VAL = 20.000 newdate = 03/07/16 CENC_VAL = 2.080 newdate = 12/13/17 REPORTING LEVEL = 2 newdate = 12/13/17 REPORTING LEVEL = 2 newdate = 12/13/17 REPORTING LEVEL = 2 newdate = 12/11/17 REPORTING LEVEL = 2 newdate = 12/11/17 REPORTING LEVEL = 2 newdate = 12/11/17 REPORTING LEVEL = 2 newdate = 12/11/17 REPORTING LEVEL = 2 newdate = 12/05/17 REPORTING LEVEL = 2 newdate = 12/05/17 REPORTING LEVEL = 2 newdate = 12/04/17 REPORTING LEVEL = 2 newdate = 12/04/17 REPORTING LEVEL = 2 newdate = 11/21/17 REPORTING LEVEL = 2 newdate = 11/21/17 REPORTING LEVEL = 2 newdate = 09/28/17 REPORTING LEVEL = 2 newdate = 09/28/17 REPORTING LEVEL = 2 newdate = 08/30/17 REPORTING LEVEL = 2 newdate = 08/30/17 REPORTING LEVEL = 2 newdate = 08/30/17 REPORTING LEVEL = 2 newdate = 08/30/17 REPORTING LEVEL = 2 newdate = 07/26/17 REPORTING LEVEL = 2 newdate = 07/26/17 REPORTING LEVEL = 2 newdate = 07/26/17 REPORTING LEVEL = 2 newdate = 07/26/17 REPORTING LEVEL = 2 newdate = 06/30/17 REPORTING LEVEL = 2 newdate = 06/30/17 REPORTING LEVEL = 2 newdate = 06/30/17 REPORTING LEVEL = 2 newdate = 06/30/17 REPORTING LEVEL = 2 newdate = 03/15/17 REPORTING LEVEL = 2 newdate = 03/15/17 REPORTING LEVEL = 2 newdate = 03/15/17 REPORTING LEVEL = 2 newdate = 03/15/17 REPORTING LEVEL = 2 newdate = 02/24/17 REPORTING LEVEL = 2 newdate = 02/24/17 REPORTING LEVEL = 2 newdate = 02/01/17 REPORTING LEVEL = 2 newdate = 02/01/17 REPORTING LEVEL = 2 newdate = 12/29/16 REPORTING LEVEL = 2 newdate = 12/29/16 REPORTING LEVEL = 2 newdate = 12/15/16 REPORTING LEVEL = 2 newdate = 12/15/16 REPORTING LEVEL = 2 newdate = 12/07/16 REPORTING LEVEL = 2 newdate = 12/07/16 REPORTING LEVEL = 2 newdate = 09/21/16 REPORTING LEVEL = 2 newdate = 09/21/16 REPORTING LEVEL = 2 newdate = 09/15/16 REPORTING LEVEL = 2 newdate = 09/15/16 REPORTING LEVEL = 2 newdate = 09/09/16 REPORTING LEVEL = 2 newdate = 09/09/16 REPORTING LEVEL = 2 newdate = 08/19/16 REPORTING LEVEL = 2 newdate = 08/19/16 REPORTING LEVEL = 2 newdate = 08/11/16 REPORTING LEVEL = 2 newdate = 08/11/16 REPORTING LEVEL = 2 newdate = 07/12/16 REPORTING LEVEL = 2 newdate = 07/12/16 REPORTING LEVEL = 2 newdate = 06/24/16 REPORTING LEVEL = 2 newdate = 06/24/16 REPORTING LEVEL = 2 newdate = 03/18/16 REPORTING LEVEL = 0.8 newdate = 03/18/16 REPORTING LEVEL = 0.8 newdate = 03/18/16 REPORTING LEVEL = 0.8 newdate = 03/18/16 REPORTING LEVEL = 0.8 newdate = 03/07/16 REPORTING LEVEL = 0.8 Y = 0
The SGPlot Procedure

False Positive & Negative Listing for CIS-ANDROSTERONE

Status Lab ID Spike Mix Reporting Level Analysis Date Result Conc. Expected Conc.
False Negative 20160840085 ERA 0601-15-04: 50 µl & ChemService 4073900: 50 µl 2 06/24/16 < 2 2.021053
  20161130024 Spex Organics EN150501025: 50 µl & ERA 0601-15-04: 50 µl 2 07/12/16 < 2 2.021053
  20162100009 ChemService 5016200: 30 µl & ChemService 5016100: 30 µl 2 09/21/16 < 2 2.014737

Updated 03/28/2018

back to table
Organic Blind Sample Program
False Positives & False Negatives
DIHYDROTESTOSTERONE
Method: 4434 Testid: 64544GM005
Link to Individual Chart

newdate = 07/25/17 falseneg = -0.01 newdate = 07/25/17 falseneg = -0.01 newdate = 09/16/16 falseneg = -0.01 newdate = 03/18/16 falseneg = -0.01 newdate = 12/11/17 CENC_VAL = 9.600 newdate = 12/05/17 CENC_VAL = 30.700 newdate = 09/05/17 CENC_VAL = 11.200 newdate = 08/30/17 CENC_VAL = 12.200 newdate = 08/30/17 CENC_VAL = 10.700 newdate = 07/28/17 CENC_VAL = 11.100 newdate = 07/26/17 CENC_VAL = 21.300 newdate = 07/13/17 CENC_VAL = 12.400 newdate = 06/02/17 CENC_VAL = 20.000 newdate = 06/02/17 CENC_VAL = 20.000 newdate = 03/15/17 CENC_VAL = 20.800 newdate = 02/01/17 CENC_VAL = 7.400 newdate = 01/13/17 CENC_VAL = 7.400 newdate = 12/29/16 CENC_VAL = 8.200 newdate = 12/05/16 CENC_VAL = 9.000 newdate = 09/15/16 CENC_VAL = 8.100 newdate = 08/31/16 CENC_VAL = 12610.00 newdate = 08/19/16 CENC_VAL = 24660.00 newdate = 08/11/16 CENC_VAL = 11000.00 newdate = 07/12/16 CENC_VAL = 8.600 newdate = 06/24/16 CENC_VAL = 8.100 newdate = 03/18/16 CENC_VAL = 7.850 newdate = 03/07/16 CENC_VAL = 8.770 newdate = 03/07/16 CENC_VAL = 5.840 newdate = 12/11/17 REPORTING LEVEL = 4 newdate = 12/05/17 REPORTING LEVEL = 4 newdate = 12/05/17 REPORTING LEVEL = 4 newdate = 09/05/17 REPORTING LEVEL = 4 newdate = 09/05/17 REPORTING LEVEL = 4 newdate = 08/30/17 REPORTING LEVEL = 4 newdate = 08/30/17 REPORTING LEVEL = 4 newdate = 08/30/17 REPORTING LEVEL = 4 newdate = 08/30/17 REPORTING LEVEL = 4 newdate = 07/28/17 REPORTING LEVEL = 4 newdate = 07/28/17 REPORTING LEVEL = 4 newdate = 07/26/17 REPORTING LEVEL = 4 newdate = 07/26/17 REPORTING LEVEL = 4 newdate = 07/25/17 REPORTING LEVEL = 4 newdate = 07/25/17 REPORTING LEVEL = 4 newdate = 07/25/17 REPORTING LEVEL = 4 newdate = 07/25/17 REPORTING LEVEL = 4 newdate = 07/13/17 REPORTING LEVEL = 4 newdate = 07/13/17 REPORTING LEVEL = 4 newdate = 06/02/17 REPORTING LEVEL = 4 newdate = 06/02/17 REPORTING LEVEL = 4 newdate = 06/02/17 REPORTING LEVEL = 4 newdate = 06/02/17 REPORTING LEVEL = 4 newdate = 03/15/17 REPORTING LEVEL = 4 newdate = 03/15/17 REPORTING LEVEL = 4 newdate = 02/01/17 REPORTING LEVEL = 4 newdate = 02/01/17 REPORTING LEVEL = 4 newdate = 01/13/17 REPORTING LEVEL = 4 newdate = 01/13/17 REPORTING LEVEL = 4 newdate = 12/29/16 REPORTING LEVEL = 4 newdate = 12/29/16 REPORTING LEVEL = 4 newdate = 12/07/16 REPORTING LEVEL = 4 newdate = 12/07/16 REPORTING LEVEL = 4 newdate = 12/05/16 REPORTING LEVEL = 4 newdate = 12/05/16 REPORTING LEVEL = 4 newdate = 09/16/16 REPORTING LEVEL = 4 newdate = 09/16/16 REPORTING LEVEL = 4 newdate = 09/15/16 REPORTING LEVEL = 4 newdate = 09/15/16 REPORTING LEVEL = 4 newdate = 08/31/16 REPORTING LEVEL = 4 newdate = 08/31/16 REPORTING LEVEL = 4 newdate = 08/19/16 REPORTING LEVEL = 4 newdate = 08/19/16 REPORTING LEVEL = 4 newdate = 08/11/16 REPORTING LEVEL = 4 newdate = 08/11/16 REPORTING LEVEL = 4 newdate = 07/12/16 REPORTING LEVEL = 4 newdate = 07/12/16 REPORTING LEVEL = 4 newdate = 06/24/16 REPORTING LEVEL = 4 newdate = 06/24/16 REPORTING LEVEL = 4 newdate = 03/18/16 REPORTING LEVEL = 4 newdate = 03/18/16 REPORTING LEVEL = 4 newdate = 03/18/16 REPORTING LEVEL = 4 newdate = 03/18/16 REPORTING LEVEL = 4 newdate = 03/07/16 REPORTING LEVEL = 4 newdate = 03/07/16 REPORTING LEVEL = 4 newdate = 03/07/16 REPORTING LEVEL = 4 Y = 0
The SGPlot Procedure

False Positive & Negative Listing for DIHYDROTESTOSTERONE

Status Lab ID Spike Mix Reporting Level Analysis Date Result Conc. Expected Conc.
False Negative 20160630047 Spex Organics EN150501025: 30 µl & Supelco LC13547: 30 µl 4 03/18/16 < 4 6
  20162020125 Spex Organics EN160621015: 30 µl & ChemService 5016200: 30 µl 4 09/16/16 < 6.5 9.978948
  20171230084 Spex Organics EN160621015: 30 µl & Abs 061416H: 30 µl 4 07/25/17 < 6.7 9.978948
  20171300147 Spex Organics EN160621015: 50 µl & Abs 061416H: 50 µl 4 07/25/17 < 5.4 16.63158

Updated 03/28/2018

back to table
Organic Blind Sample Program
False Positives & False Negatives
EPITESTOSTERONE
Method: 4434 Testid: 64537GM005
Link to Individual Chart

newdate = 07/25/17 falseneg = -0.01 newdate = 07/25/17 falseneg = -0.01 newdate = 06/02/17 falseneg = -0.01 newdate = 06/02/17 falseneg = -0.01 newdate = 12/11/17 CENC_VAL = 7.100 newdate = 12/05/17 CENC_VAL = 16.600 newdate = 09/05/17 CENC_VAL = 5.500 newdate = 08/30/17 CENC_VAL = 8.300 newdate = 08/30/17 CENC_VAL = 6.300 newdate = 07/28/17 CENC_VAL = 5.100 newdate = 07/26/17 CENC_VAL = 10.000 newdate = 07/13/17 CENC_VAL = 5.200 newdate = 03/15/17 CENC_VAL = 11.600 newdate = 02/01/17 CENC_VAL = 3.500 newdate = 01/13/17 CENC_VAL = 4.000 newdate = 12/29/16 CENC_VAL = 6.000 newdate = 12/05/16 CENC_VAL = 2.600 newdate = 09/16/16 CENC_VAL = 4.500 newdate = 09/15/16 CENC_VAL = 3.800 newdate = 08/31/16 CENC_VAL = 7240.000 newdate = 08/19/16 CENC_VAL = 11230.00 newdate = 08/11/16 CENC_VAL = 5215.000 newdate = 07/12/16 CENC_VAL = 3.100 newdate = 06/24/16 CENC_VAL = 2.700 newdate = 03/18/16 CENC_VAL = 1.940 newdate = 03/18/16 CENC_VAL = 1.930 newdate = 03/07/16 CENC_VAL = 2.490 newdate = 03/07/16 CENC_VAL = 1.170 newdate = 12/11/17 REPORTING LEVEL = 2 newdate = 12/05/17 REPORTING LEVEL = 2 newdate = 12/05/17 REPORTING LEVEL = 2 newdate = 09/05/17 REPORTING LEVEL = 2 newdate = 09/05/17 REPORTING LEVEL = 2 newdate = 08/30/17 REPORTING LEVEL = 2 newdate = 08/30/17 REPORTING LEVEL = 2 newdate = 08/30/17 REPORTING LEVEL = 2 newdate = 08/30/17 REPORTING LEVEL = 2 newdate = 07/28/17 REPORTING LEVEL = 2 newdate = 07/28/17 REPORTING LEVEL = 2 newdate = 07/26/17 REPORTING LEVEL = 2 newdate = 07/26/17 REPORTING LEVEL = 2 newdate = 07/25/17 REPORTING LEVEL = 2 newdate = 07/25/17 REPORTING LEVEL = 2 newdate = 07/25/17 REPORTING LEVEL = 2 newdate = 07/25/17 REPORTING LEVEL = 2 newdate = 07/13/17 REPORTING LEVEL = 2 newdate = 07/13/17 REPORTING LEVEL = 2 newdate = 06/02/17 REPORTING LEVEL = 2 newdate = 06/02/17 REPORTING LEVEL = 2 newdate = 06/02/17 REPORTING LEVEL = 2 newdate = 06/02/17 REPORTING LEVEL = 2 newdate = 03/15/17 REPORTING LEVEL = 2 newdate = 03/15/17 REPORTING LEVEL = 2 newdate = 02/01/17 REPORTING LEVEL = 2 newdate = 02/01/17 REPORTING LEVEL = 2 newdate = 01/13/17 REPORTING LEVEL = 2 newdate = 01/13/17 REPORTING LEVEL = 2 newdate = 12/29/16 REPORTING LEVEL = 2 newdate = 12/29/16 REPORTING LEVEL = 2 newdate = 12/07/16 REPORTING LEVEL = 2 newdate = 12/07/16 REPORTING LEVEL = 2 newdate = 12/05/16 REPORTING LEVEL = 2 newdate = 12/05/16 REPORTING LEVEL = 2 newdate = 09/16/16 REPORTING LEVEL = 2 newdate = 09/16/16 REPORTING LEVEL = 2 newdate = 09/15/16 REPORTING LEVEL = 2 newdate = 09/15/16 REPORTING LEVEL = 2 newdate = 08/31/16 REPORTING LEVEL = 2 newdate = 08/31/16 REPORTING LEVEL = 2 newdate = 08/19/16 REPORTING LEVEL = 2 newdate = 08/19/16 REPORTING LEVEL = 2 newdate = 08/11/16 REPORTING LEVEL = 2 newdate = 08/11/16 REPORTING LEVEL = 2 newdate = 07/12/16 REPORTING LEVEL = 2 newdate = 07/12/16 REPORTING LEVEL = 2 newdate = 06/24/16 REPORTING LEVEL = 2 newdate = 06/24/16 REPORTING LEVEL = 2 newdate = 03/18/16 REPORTING LEVEL = 2 newdate = 03/18/16 REPORTING LEVEL = 2 newdate = 03/18/16 REPORTING LEVEL = 2 newdate = 03/18/16 REPORTING LEVEL = 2 newdate = 03/07/16 REPORTING LEVEL = 2 newdate = 03/07/16 REPORTING LEVEL = 2 newdate = 03/07/16 REPORTING LEVEL = 2 Y = 0
The SGPlot Procedure

False Positive & Negative Listing for EPITESTOSTERONE

Status Lab ID Spike Mix Reporting Level Analysis Date Result Conc. Expected Conc.
False Negative 20170320040 Abs 052616: 50 µl & Abs 061416H: 50 µl 2 06/02/17 < 4.1 8.365263
  20170320041 Abs 052616: 50 µl & Abs 061416H: 50 µl 2 06/02/17 < 2 8.365263
  20171230084 Spex Organics EN160621015: 30 µl & Abs 061416H: 30 µl 2 07/25/17 < 4.1 5.096842
  20171300147 Spex Organics EN160621015: 50 µl & Abs 061416H: 50 µl 2 07/25/17 < 6.1 8.494737

Updated 03/28/2018

back to table
Organic Blind Sample Program
False Positives & False Negatives
EQUILENIN
Method: 4434 Testid: 64538GM005
Link to Individual Chart

newdate = 09/21/16 falsepos = 2.3 newdate = 12/11/17 CENC_VAL = 15.500 newdate = 12/05/17 CENC_VAL = 10.200 newdate = 09/28/17 CENC_VAL = 4.200 newdate = 08/30/17 CENC_VAL = 9.300 newdate = 07/26/17 CENC_VAL = 4.000 newdate = 03/15/17 CENC_VAL = 5.500 newdate = 02/24/17 CENC_VAL = 8.300 newdate = 02/01/17 CENC_VAL = 5.500 newdate = 09/15/16 CENC_VAL = 5.100 newdate = 09/09/16 CENC_VAL = 5.900 newdate = 08/19/16 CENC_VAL = 7.700 newdate = 03/07/16 CENC_VAL = 3.770 newdate = 12/11/17 REPORTING LEVEL = 2 newdate = 12/05/17 REPORTING LEVEL = 2 newdate = 12/05/17 REPORTING LEVEL = 2 newdate = 09/28/17 REPORTING LEVEL = 2 newdate = 09/28/17 REPORTING LEVEL = 2 newdate = 08/30/17 REPORTING LEVEL = 2 newdate = 08/30/17 REPORTING LEVEL = 2 newdate = 07/26/17 REPORTING LEVEL = 2 newdate = 07/26/17 REPORTING LEVEL = 2 newdate = 03/15/17 REPORTING LEVEL = 2 newdate = 03/15/17 REPORTING LEVEL = 2 newdate = 02/24/17 REPORTING LEVEL = 2 newdate = 02/24/17 REPORTING LEVEL = 2 newdate = 02/01/17 REPORTING LEVEL = 2 newdate = 02/01/17 REPORTING LEVEL = 2 newdate = 12/07/16 REPORTING LEVEL = 2 newdate = 12/07/16 REPORTING LEVEL = 2 newdate = 09/21/16 REPORTING LEVEL = 2 newdate = 09/21/16 REPORTING LEVEL = 2 newdate = 09/15/16 REPORTING LEVEL = 2 newdate = 09/15/16 REPORTING LEVEL = 2 newdate = 09/09/16 REPORTING LEVEL = 2 newdate = 09/09/16 REPORTING LEVEL = 2 newdate = 08/19/16 REPORTING LEVEL = 2 newdate = 08/19/16 REPORTING LEVEL = 2 newdate = 03/07/16 REPORTING LEVEL = 2
The SGPlot Procedure

False Positive & Negative Listing for EQUILENIN

Status Lab ID Spike Mix Reporting Level Analysis Date Result Conc. Expected Conc.
False Positive 20162100009 ChemService 5016200: 30 µl & ChemService 5016100: 30 µl 2 09/21/16 E 2.3 0

Updated 03/28/2018

back to table
Organic Blind Sample Program
False Positives & False Negatives
EQUILIN
Method: 4434 Testid: 64539GM005
Link to Individual Chart

newdate = 07/26/17 falseneg = -0.01 newdate = 03/15/17 falseneg = -0.01 newdate = 12/29/16 falseneg = -0.01 newdate = 09/15/16 falseneg = -0.01 newdate = 09/09/16 falseneg = -0.01 newdate = 03/18/16 falseneg = -0.01 newdate = 03/18/16 falseneg = -0.01 newdate = 03/07/16 falseneg = -0.01 newdate = 12/13/17 CENC_VAL = 43.500 newdate = 12/13/17 CENC_VAL = 16.300 newdate = 12/11/17 CENC_VAL = 82.300 newdate = 09/28/17 CENC_VAL = 17.200 newdate = 08/30/17 CENC_VAL = 27.200 newdate = 08/30/17 CENC_VAL = 20.500 newdate = 07/26/17 CENC_VAL = 25.700 newdate = 06/30/17 CENC_VAL = 26.000 newdate = 06/30/17 CENC_VAL = 19.400 newdate = 03/15/17 CENC_VAL = 27.900 newdate = 02/24/17 CENC_VAL = 13.600 newdate = 02/01/17 CENC_VAL = 12.600 newdate = 12/15/16 CENC_VAL = 20.900 newdate = 09/21/16 CENC_VAL = 13.900 newdate = 08/19/16 CENC_VAL = 44.600 newdate = 08/11/16 CENC_VAL = 27.500 newdate = 06/24/16 CENC_VAL = 13.100 newdate = 06/24/16 CENC_VAL = 16.700 newdate = 12/13/17 REPORTING LEVEL = 16 newdate = 12/13/17 REPORTING LEVEL = 16 newdate = 12/13/17 REPORTING LEVEL = 16 newdate = 12/11/17 REPORTING LEVEL = 16 newdate = 12/11/17 REPORTING LEVEL = 16 newdate = 09/28/17 REPORTING LEVEL = 16 newdate = 09/28/17 REPORTING LEVEL = 16 newdate = 08/30/17 REPORTING LEVEL = 16 newdate = 08/30/17 REPORTING LEVEL = 16 newdate = 08/30/17 REPORTING LEVEL = 16 newdate = 08/30/17 REPORTING LEVEL = 16 newdate = 07/26/17 REPORTING LEVEL = 16 newdate = 07/26/17 REPORTING LEVEL = 16 newdate = 07/26/17 REPORTING LEVEL = 16 newdate = 07/26/17 REPORTING LEVEL = 16 newdate = 06/30/17 REPORTING LEVEL = 16 newdate = 06/30/17 REPORTING LEVEL = 16 newdate = 06/30/17 REPORTING LEVEL = 16 newdate = 06/30/17 REPORTING LEVEL = 16 newdate = 03/15/17 REPORTING LEVEL = 16 newdate = 03/15/17 REPORTING LEVEL = 16 newdate = 03/15/17 REPORTING LEVEL = 16 newdate = 03/15/17 REPORTING LEVEL = 16 newdate = 02/24/17 REPORTING LEVEL = 16 newdate = 02/24/17 REPORTING LEVEL = 16 newdate = 02/01/17 REPORTING LEVEL = 16 newdate = 02/01/17 REPORTING LEVEL = 16 newdate = 12/29/16 REPORTING LEVEL = 16 newdate = 12/29/16 REPORTING LEVEL = 16 newdate = 12/15/16 REPORTING LEVEL = 16 newdate = 12/15/16 REPORTING LEVEL = 16 newdate = 12/07/16 REPORTING LEVEL = 16 newdate = 12/07/16 REPORTING LEVEL = 16 newdate = 09/21/16 REPORTING LEVEL = 16 newdate = 09/21/16 REPORTING LEVEL = 16 newdate = 09/15/16 REPORTING LEVEL = 16 newdate = 09/15/16 REPORTING LEVEL = 16 newdate = 09/09/16 REPORTING LEVEL = 16 newdate = 09/09/16 REPORTING LEVEL = 16 newdate = 08/19/16 REPORTING LEVEL = 16 newdate = 08/19/16 REPORTING LEVEL = 16 newdate = 08/11/16 REPORTING LEVEL = 16 newdate = 08/11/16 REPORTING LEVEL = 16 newdate = 06/24/16 REPORTING LEVEL = 16 newdate = 06/24/16 REPORTING LEVEL = 16 newdate = 06/24/16 REPORTING LEVEL = 16 newdate = 06/24/16 REPORTING LEVEL = 16 newdate = 03/18/16 REPORTING LEVEL = 8 newdate = 03/18/16 REPORTING LEVEL = 8 newdate = 03/18/16 REPORTING LEVEL = 8 newdate = 03/18/16 REPORTING LEVEL = 8 newdate = 03/07/16 REPORTING LEVEL = 8 Y = 0
The SGPlot Procedure

False Positive & Negative Listing for EQUILIN

Status Lab ID Spike Mix Reporting Level Analysis Date Result Conc. Expected Conc.
False Negative 20160070058 ChemService 4073900: 30 µl & Abs 041515: 30 µl 8 03/07/16 < 8 12.10737
  20160430110 Supelco LC13547: 30 µl & ChemService 4073900: 30 µl 8 03/18/16 < 8 12.10737
  20160560045 Crescent 04EE007: 30 µl & Spex Organics EN150501025: 30 µl 8 03/18/16 < 8 11.87368
  20161820010 ChemService 5016200: 30 µl & Supelco LC20140V: 30 µl 16 09/09/16 < 16 20.08421
  20161960002 Supelco LC20140V: 30 µl & Spex Organics EN160621015: 30 µl 16 09/15/16 < 16 20.08421
  20162800003 ChemService 5016100: 30 µl & Abs 052616: 30 µl 16 12/29/16 < 16 20.19158
  20163630037 ChemService 5016200: 30 µl & Supelco LC20140V: 30 µl 16 03/15/17 < 20 20.08421
  20171510081 Supelco LC20140V: 30 µl & ChemService 5016200: 30 µl 16 07/26/17 < 20 20.08421

Updated 03/28/2018

back to table
Organic Blind Sample Program
False Positives & False Negatives
ESTRIOL
Method: 4434 Testid: 64540GM005
Link to Individual Chart

newdate = 06/02/17 falseneg = -0.01 newdate = 08/31/16 falseneg = -0.01 newdate = 12/13/17 CENC_VAL = 23.400 newdate = 12/13/17 CENC_VAL = 2.100 newdate = 12/11/17 CENC_VAL = 12.600 newdate = 09/28/17 CENC_VAL = 7.700 newdate = 09/05/17 CENC_VAL = 4.900 newdate = 07/28/17 CENC_VAL = 6.700 newdate = 07/26/17 CENC_VAL = 3.700 newdate = 07/25/17 CENC_VAL = 5.800 newdate = 07/25/17 CENC_VAL = 3.400 newdate = 07/13/17 CENC_VAL = 5.900 newdate = 06/30/17 CENC_VAL = 11.900 newdate = 06/30/17 CENC_VAL = 8.100 newdate = 06/02/17 CENC_VAL = 5.800 newdate = 03/15/17 CENC_VAL = 4.300 newdate = 02/24/17 CENC_VAL = 6.800 newdate = 01/13/17 CENC_VAL = 4.000 newdate = 12/15/16 CENC_VAL = 7.300 newdate = 12/05/16 CENC_VAL = 5.200 newdate = 09/21/16 CENC_VAL = 5.300 newdate = 09/16/16 CENC_VAL = 4.900 newdate = 09/09/16 CENC_VAL = 4.600 newdate = 06/24/16 CENC_VAL = 4.400 newdate = 06/24/16 CENC_VAL = 4.200 newdate = 03/18/16 CENC_VAL = 3.140 newdate = 03/18/16 CENC_VAL = 3.260 newdate = 03/07/16 CENC_VAL = 1.570 newdate = 12/13/17 REPORTING LEVEL = 2 newdate = 12/13/17 REPORTING LEVEL = 2 newdate = 12/13/17 REPORTING LEVEL = 2 newdate = 12/11/17 REPORTING LEVEL = 2 newdate = 12/11/17 REPORTING LEVEL = 2 newdate = 09/28/17 REPORTING LEVEL = 2 newdate = 09/28/17 REPORTING LEVEL = 2 newdate = 09/05/17 REPORTING LEVEL = 2 newdate = 09/05/17 REPORTING LEVEL = 2 newdate = 07/28/17 REPORTING LEVEL = 2 newdate = 07/28/17 REPORTING LEVEL = 2 newdate = 07/26/17 REPORTING LEVEL = 2 newdate = 07/26/17 REPORTING LEVEL = 2 newdate = 07/25/17 REPORTING LEVEL = 2 newdate = 07/25/17 REPORTING LEVEL = 2 newdate = 07/25/17 REPORTING LEVEL = 2 newdate = 07/25/17 REPORTING LEVEL = 2 newdate = 07/13/17 REPORTING LEVEL = 2 newdate = 07/13/17 REPORTING LEVEL = 2 newdate = 06/30/17 REPORTING LEVEL = 2 newdate = 06/30/17 REPORTING LEVEL = 2 newdate = 06/30/17 REPORTING LEVEL = 2 newdate = 06/30/17 REPORTING LEVEL = 2 newdate = 06/02/17 REPORTING LEVEL = 2 newdate = 06/02/17 REPORTING LEVEL = 2 newdate = 06/02/17 REPORTING LEVEL = 2 newdate = 06/02/17 REPORTING LEVEL = 2 newdate = 03/15/17 REPORTING LEVEL = 2 newdate = 03/15/17 REPORTING LEVEL = 2 newdate = 02/24/17 REPORTING LEVEL = 2 newdate = 02/24/17 REPORTING LEVEL = 2 newdate = 01/13/17 REPORTING LEVEL = 2 newdate = 01/13/17 REPORTING LEVEL = 2 newdate = 12/15/16 REPORTING LEVEL = 2 newdate = 12/15/16 REPORTING LEVEL = 2 newdate = 12/07/16 REPORTING LEVEL = 2 newdate = 12/07/16 REPORTING LEVEL = 2 newdate = 12/05/16 REPORTING LEVEL = 2 newdate = 12/05/16 REPORTING LEVEL = 2 newdate = 09/21/16 REPORTING LEVEL = 2 newdate = 09/21/16 REPORTING LEVEL = 2 newdate = 09/16/16 REPORTING LEVEL = 2 newdate = 09/16/16 REPORTING LEVEL = 2 newdate = 09/09/16 REPORTING LEVEL = 2 newdate = 09/09/16 REPORTING LEVEL = 2 newdate = 08/31/16 REPORTING LEVEL = 2 newdate = 08/31/16 REPORTING LEVEL = 2 newdate = 06/24/16 REPORTING LEVEL = 2 newdate = 06/24/16 REPORTING LEVEL = 2 newdate = 06/24/16 REPORTING LEVEL = 2 newdate = 06/24/16 REPORTING LEVEL = 2 newdate = 03/18/16 REPORTING LEVEL = 2 newdate = 03/18/16 REPORTING LEVEL = 2 newdate = 03/18/16 REPORTING LEVEL = 2 newdate = 03/18/16 REPORTING LEVEL = 2 newdate = 03/07/16 REPORTING LEVEL = 2 Y = 0
The SGPlot Procedure

False Positive & Negative Listing for ESTRIOL

Status Lab ID Spike Mix Reporting Level Analysis Date Result Conc. Expected Conc.
False Negative 20161740282 Spex Organics TS160420010: 50 µl & ChemService 5016200: 50 µl 2 08/31/16 < 5.3 8.336842
  20170320041 Abs 052616: 50 µl & Abs 061416H: 50 µl 2 06/02/17 < 5.7 8.330526

Updated 03/28/2018

back to table
Organic Blind Sample Program
False Positives & False Negatives
ESTRONE
Method: 4434 Testid: 64541GM005
Link to Individual Chart

newdate = 08/30/17 falseneg = -0.01 newdate = 07/26/17 falseneg = -0.01 newdate = 07/25/17 falseneg = -0.01 newdate = 06/02/17 falseneg = -0.01 newdate = 06/02/17 falseneg = -0.01 newdate = 07/12/16 falseneg = -0.01 newdate = 03/18/16 falseneg = -0.01 newdate = 03/18/16 falseneg = -0.01 newdate = 12/13/17 CENC_VAL = 17.300 newdate = 12/13/17 CENC_VAL = 2.100 newdate = 12/11/17 CENC_VAL = 16.700 newdate = 12/11/17 CENC_VAL = 12.100 newdate = 12/05/17 CENC_VAL = 13.100 newdate = 12/04/17 CENC_VAL = 2.300 newdate = 11/21/17 CENC_VAL = 3.500 newdate = 09/05/17 CENC_VAL = 2.000 newdate = 08/30/17 CENC_VAL = 4.500 newdate = 07/28/17 CENC_VAL = 1.900 newdate = 07/25/17 CENC_VAL = 4.600 newdate = 07/13/17 CENC_VAL = 2.400 newdate = 03/15/17 CENC_VAL = 4.100 newdate = 02/01/17 CENC_VAL = 1.400 newdate = 01/13/17 CENC_VAL = 1.600 newdate = 12/29/16 CENC_VAL = 1.400 newdate = 12/05/16 CENC_VAL = 2.500 newdate = 09/16/16 CENC_VAL = 1.300 newdate = 09/15/16 CENC_VAL = 2.400 newdate = 08/31/16 CENC_VAL = 1586.000 newdate = 08/19/16 CENC_VAL = 2200.000 newdate = 08/11/16 CENC_VAL = 1767.000 newdate = 06/24/16 CENC_VAL = 1.900 newdate = 03/07/16 CENC_VAL = 1.190 newdate = 12/13/17 REPORTING LEVEL = 2 newdate = 12/13/17 REPORTING LEVEL = 2 newdate = 12/13/17 REPORTING LEVEL = 2 newdate = 12/11/17 REPORTING LEVEL = 2 newdate = 12/11/17 REPORTING LEVEL = 2 newdate = 12/11/17 REPORTING LEVEL = 2 newdate = 12/11/17 REPORTING LEVEL = 2 newdate = 12/05/17 REPORTING LEVEL = 2 newdate = 12/05/17 REPORTING LEVEL = 2 newdate = 12/04/17 REPORTING LEVEL = 2 newdate = 12/04/17 REPORTING LEVEL = 2 newdate = 11/21/17 REPORTING LEVEL = 2 newdate = 11/21/17 REPORTING LEVEL = 2 newdate = 09/05/17 REPORTING LEVEL = 2 newdate = 09/05/17 REPORTING LEVEL = 2 newdate = 08/30/17 REPORTING LEVEL = 2 newdate = 08/30/17 REPORTING LEVEL = 2 newdate = 08/30/17 REPORTING LEVEL = 2 newdate = 08/30/17 REPORTING LEVEL = 2 newdate = 07/28/17 REPORTING LEVEL = 2 newdate = 07/28/17 REPORTING LEVEL = 2 newdate = 07/26/17 REPORTING LEVEL = 2 newdate = 07/26/17 REPORTING LEVEL = 2 newdate = 07/25/17 REPORTING LEVEL = 2 newdate = 07/25/17 REPORTING LEVEL = 2 newdate = 07/25/17 REPORTING LEVEL = 2 newdate = 07/25/17 REPORTING LEVEL = 2 newdate = 07/13/17 REPORTING LEVEL = 2 newdate = 07/13/17 REPORTING LEVEL = 2 newdate = 06/02/17 REPORTING LEVEL = 2 newdate = 06/02/17 REPORTING LEVEL = 2 newdate = 06/02/17 REPORTING LEVEL = 2 newdate = 06/02/17 REPORTING LEVEL = 2 newdate = 03/15/17 REPORTING LEVEL = 2 newdate = 03/15/17 REPORTING LEVEL = 2 newdate = 02/01/17 REPORTING LEVEL = 2 newdate = 02/01/17 REPORTING LEVEL = 2 newdate = 01/13/17 REPORTING LEVEL = 2 newdate = 01/13/17 REPORTING LEVEL = 2 newdate = 12/29/16 REPORTING LEVEL = 2 newdate = 12/29/16 REPORTING LEVEL = 2 newdate = 12/07/16 REPORTING LEVEL = 2 newdate = 12/07/16 REPORTING LEVEL = 2 newdate = 12/05/16 REPORTING LEVEL = 2 newdate = 12/05/16 REPORTING LEVEL = 2 newdate = 09/16/16 REPORTING LEVEL = 2 newdate = 09/16/16 REPORTING LEVEL = 2 newdate = 09/15/16 REPORTING LEVEL = 2 newdate = 09/15/16 REPORTING LEVEL = 2 newdate = 08/31/16 REPORTING LEVEL = 2 newdate = 08/31/16 REPORTING LEVEL = 2 newdate = 08/19/16 REPORTING LEVEL = 2 newdate = 08/19/16 REPORTING LEVEL = 2 newdate = 08/11/16 REPORTING LEVEL = 2 newdate = 08/11/16 REPORTING LEVEL = 2 newdate = 07/12/16 REPORTING LEVEL = 2 newdate = 07/12/16 REPORTING LEVEL = 2 newdate = 06/24/16 REPORTING LEVEL = 2 newdate = 06/24/16 REPORTING LEVEL = 2 newdate = 03/18/16 REPORTING LEVEL = 0.8 newdate = 03/18/16 REPORTING LEVEL = 0.8 newdate = 03/18/16 REPORTING LEVEL = 0.8 newdate = 03/18/16 REPORTING LEVEL = 0.8 newdate = 03/07/16 REPORTING LEVEL = 0.8 Y = 0
The SGPlot Procedure

False Positive & Negative Listing for ESTRONE

Status Lab ID Spike Mix Reporting Level Analysis Date Result Conc. Expected Conc.
False Negative 20160430110 Supelco LC13547: 30 µl & ChemService 4073900: 30 µl 0.8 03/18/16 < 0.8 1.2
  20160630047 Spex Organics EN150501025: 30 µl & Supelco LC13547: 30 µl 0.8 03/18/16 < 0.8 1.2
  20161130024 Spex Organics EN150501025: 50 µl & ERA 0601-15-04: 50 µl 2 07/12/16 < 2 2.021053
  20170320040 Abs 052616: 50 µl & Abs 061416H: 50 µl 2 06/02/17 < 2 3.391579
  20170320041 Abs 052616: 50 µl & Abs 061416H: 50 µl 2 06/02/17 < 2 3.391579
  20171230084 Spex Organics EN160621015: 30 µl & Abs 061416H: 30 µl 2 07/25/17 < 2 2.002105
  20171380004 ChemService 5016100: 80 µl & Abs 052616: 80 µl 2 07/26/17 < 4 5.426527
  20171790208 ChemService 5016100: 50 µl & Abs 052616: 50 µl 2 08/30/17 < 2 3.391579

Updated 03/28/2018

back to table
Organic Blind Sample Program
False Positives & False Negatives
MESTRANOL
Method: 4434 Testid: 64542GM005
Link to Individual Chart

newdate = 08/30/17 falseneg = -0.01 newdate = 08/30/17 falseneg = -0.01 newdate = 07/28/17 falseneg = -0.01 newdate = 07/13/17 falseneg = -0.01 newdate = 06/02/17 falseneg = -0.01 newdate = 06/02/17 falseneg = -0.01 newdate = 03/15/17 falseneg = -0.01 newdate = 02/01/17 falseneg = -0.01 newdate = 12/29/16 falseneg = -0.01 newdate = 12/05/16 falseneg = -0.01 newdate = 09/16/16 falseneg = -0.01 newdate = 09/15/16 falseneg = -0.01 newdate = 03/18/16 falseneg = -0.01 newdate = 03/18/16 falseneg = -0.01 newdate = 03/07/16 falseneg = -0.01 newdate = 03/07/16 falsepos = 23.8 newdate = 12/13/17 CENC_VAL = 9.800 newdate = 12/13/17 CENC_VAL = 1.200 newdate = 12/11/17 CENC_VAL = 6.100 newdate = 09/05/17 CENC_VAL = 1.400 newdate = 07/26/17 CENC_VAL = 2.700 newdate = 07/25/17 CENC_VAL = 2.900 newdate = 07/25/17 CENC_VAL = 4.000 newdate = 01/13/17 CENC_VAL = 0.900 newdate = 06/24/16 CENC_VAL = 20.000 newdate = 06/24/16 CENC_VAL = 20.000 newdate = 12/13/17 REPORTING LEVEL = 1.6 newdate = 12/13/17 REPORTING LEVEL = 1.6 newdate = 12/13/17 REPORTING LEVEL = 1.6 newdate = 12/11/17 REPORTING LEVEL = 1.6 newdate = 12/11/17 REPORTING LEVEL = 1.6 newdate = 09/05/17 REPORTING LEVEL = 1.6 newdate = 09/05/17 REPORTING LEVEL = 1.6 newdate = 08/30/17 REPORTING LEVEL = 1.6 newdate = 08/30/17 REPORTING LEVEL = 1.6 newdate = 08/30/17 REPORTING LEVEL = 1.6 newdate = 08/30/17 REPORTING LEVEL = 1.6 newdate = 07/28/17 REPORTING LEVEL = 1.6 newdate = 07/28/17 REPORTING LEVEL = 1.6 newdate = 07/26/17 REPORTING LEVEL = 1.6 newdate = 07/26/17 REPORTING LEVEL = 1.6 newdate = 07/25/17 REPORTING LEVEL = 1.6 newdate = 07/25/17 REPORTING LEVEL = 1.6 newdate = 07/25/17 REPORTING LEVEL = 1.6 newdate = 07/25/17 REPORTING LEVEL = 1.6 newdate = 07/13/17 REPORTING LEVEL = 1.6 newdate = 07/13/17 REPORTING LEVEL = 1.6 newdate = 06/02/17 REPORTING LEVEL = 1.6 newdate = 06/02/17 REPORTING LEVEL = 1.6 newdate = 06/02/17 REPORTING LEVEL = 1.6 newdate = 06/02/17 REPORTING LEVEL = 1.6 newdate = 03/15/17 REPORTING LEVEL = 1.6 newdate = 03/15/17 REPORTING LEVEL = 1.6 newdate = 02/01/17 REPORTING LEVEL = 1.6 newdate = 02/01/17 REPORTING LEVEL = 1.6 newdate = 01/13/17 REPORTING LEVEL = 1.6 newdate = 01/13/17 REPORTING LEVEL = 1.6 newdate = 12/29/16 REPORTING LEVEL = 1.6 newdate = 12/29/16 REPORTING LEVEL = 1.6 newdate = 12/07/16 REPORTING LEVEL = 1.6 newdate = 12/07/16 REPORTING LEVEL = 1.6 newdate = 12/05/16 REPORTING LEVEL = 1.6 newdate = 12/05/16 REPORTING LEVEL = 1.6 newdate = 09/16/16 REPORTING LEVEL = 1.6 newdate = 09/16/16 REPORTING LEVEL = 1.6 newdate = 09/15/16 REPORTING LEVEL = 1.6 newdate = 09/15/16 REPORTING LEVEL = 1.6 newdate = 06/24/16 REPORTING LEVEL = 1.6 newdate = 06/24/16 REPORTING LEVEL = 1.6 newdate = 06/24/16 REPORTING LEVEL = 1.6 newdate = 06/24/16 REPORTING LEVEL = 1.6 newdate = 03/18/16 REPORTING LEVEL = 0.8 newdate = 03/18/16 REPORTING LEVEL = 0.8 newdate = 03/18/16 REPORTING LEVEL = 0.8 newdate = 03/18/16 REPORTING LEVEL = 0.8 newdate = 03/07/16 REPORTING LEVEL = 0.8 newdate = 03/07/16 REPORTING LEVEL = 0.8 newdate = 03/07/16 REPORTING LEVEL = 0.8 Y = 0
The SGPlot Procedure

False Positive & Negative Listing for MESTRANOL

Status Lab ID Spike Mix Reporting Level Analysis Date Result Conc. Expected Conc.
False Negative 20160070058 ChemService 4073900: 30 µl & Abs 041515: 30 µl 0.8 03/07/16 < 0.8 1.2
  20160430110 Supelco LC13547: 30 µl & ChemService 4073900: 30 µl 0.8 03/18/16 < 0.8 1.2
  20160560045 Crescent 04EE007: 30 µl & Spex Organics EN150501025: 30 µl 0.8 03/18/16 < 0.8 1.2
  20161960002 Supelco LC20140V: 30 µl & Spex Organics EN160621015: 30 µl 1.6 09/15/16 < 1.6 1.995789
  20162020125 Spex Organics EN160621015: 30 µl & ChemService 5016200: 30 µl 1.6 09/16/16 < 1.6 1.995789
  20162300273 Abs 052616: 30 µl & Abs 061416H: 30 µl 1.6 12/05/16 < 1.6 2.026737
  20162800003 ChemService 5016100: 30 µl & Abs 052616: 30 µl 1.6 12/29/16 < 1.6 2.026737
  20163220167 Supelco LC20140V: 30 µl & Abs 052616: 30 µl 1.6 02/01/17 < 1.6 2.026737
  20170110049 ChemService 5016100: 80 µl & Abs 052616: 80 µl 1.6 03/15/17 < 2.1 5.404632
  20170320040 Abs 052616: 50 µl & Abs 061416H: 50 µl 1.6 06/02/17 < 2 3.377895
  20170320041 Abs 052616: 50 µl & Abs 061416H: 50 µl 1.6 06/02/17 < 2 3.377895
  20171020122 Abs 052616: 50 µl & ChemService 5016200: 50 µl 1.6 07/13/17 < 1.8 3.377895
  20171580162 Spex Organics EN160621015: 50 µl & Abs 061416H: 50 µl 1.6 07/28/17 < 2 3.326316
  20171720141 Supelco LC20140V: 80 µl & Spex Organics EN160621015: 80 µl 1.6 08/30/17 < 1.9 5.322105
  20171790208 ChemService 5016100: 50 µl & Abs 052616: 50 µl 1.6 08/30/17 < 1.6 3.377895
False Positive 20160280054 Abs 041515: 50 µl & ERA 0601-15-04: 50 µl 0.8 03/07/16 23.8 0

Updated 03/28/2018

back to table
Organic Blind Sample Program
False Positives & False Negatives
NORETHINDRONE
Method: 4434 Testid: 64531GM005
Link to Individual Chart

newdate = 09/28/17 falseneg = -0.01 newdate = 08/30/17 falseneg = -0.01 newdate = 07/26/17 falseneg = -0.01 newdate = 06/30/17 falseneg = -0.01 newdate = 09/15/16 falseneg = -0.01 newdate = 09/09/16 falseneg = -0.01 newdate = 08/11/16 falseneg = -0.01 newdate = 03/18/16 falseneg = -0.01 newdate = 03/18/16 falseneg = -0.01 newdate = 03/07/16 falseneg = -0.01 newdate = 03/07/16 falseneg = -0.01 newdate = 12/11/17 CENC_VAL = 18.700 newdate = 12/05/17 CENC_VAL = 13.300 newdate = 12/04/17 CENC_VAL = 2.300 newdate = 11/21/17 CENC_VAL = 3.100 newdate = 08/30/17 CENC_VAL = 3.100 newdate = 07/26/17 CENC_VAL = 3.000 newdate = 06/30/17 CENC_VAL = 5.400 newdate = 03/15/17 CENC_VAL = 4.600 newdate = 03/15/17 CENC_VAL = 1.500 newdate = 02/24/17 CENC_VAL = 1.400 newdate = 02/01/17 CENC_VAL = 1.800 newdate = 12/29/16 CENC_VAL = 1.900 newdate = 12/15/16 CENC_VAL = 2.700 newdate = 09/21/16 CENC_VAL = 1.300 newdate = 08/19/16 CENC_VAL = 3.300 newdate = 07/12/16 CENC_VAL = 3.000 newdate = 06/24/16 CENC_VAL = 2.900 newdate = 12/11/17 REPORTING LEVEL = 1.6 newdate = 12/05/17 REPORTING LEVEL = 1.6 newdate = 12/05/17 REPORTING LEVEL = 1.6 newdate = 12/04/17 REPORTING LEVEL = 1.6 newdate = 12/04/17 REPORTING LEVEL = 1.6 newdate = 11/21/17 REPORTING LEVEL = 1.6 newdate = 11/21/17 REPORTING LEVEL = 1.6 newdate = 09/28/17 REPORTING LEVEL = 1.6 newdate = 09/28/17 REPORTING LEVEL = 1.6 newdate = 08/30/17 REPORTING LEVEL = 1.6 newdate = 08/30/17 REPORTING LEVEL = 1.6 newdate = 08/30/17 REPORTING LEVEL = 1.6 newdate = 08/30/17 REPORTING LEVEL = 1.6 newdate = 07/26/17 REPORTING LEVEL = 1.6 newdate = 07/26/17 REPORTING LEVEL = 1.6 newdate = 07/26/17 REPORTING LEVEL = 1.6 newdate = 07/26/17 REPORTING LEVEL = 1.6 newdate = 06/30/17 REPORTING LEVEL = 1.6 newdate = 06/30/17 REPORTING LEVEL = 1.6 newdate = 06/30/17 REPORTING LEVEL = 1.6 newdate = 06/30/17 REPORTING LEVEL = 1.6 newdate = 03/15/17 REPORTING LEVEL = 1.6 newdate = 03/15/17 REPORTING LEVEL = 1.6 newdate = 03/15/17 REPORTING LEVEL = 1.6 newdate = 03/15/17 REPORTING LEVEL = 1.6 newdate = 02/24/17 REPORTING LEVEL = 1.6 newdate = 02/24/17 REPORTING LEVEL = 1.6 newdate = 02/01/17 REPORTING LEVEL = 1.6 newdate = 02/01/17 REPORTING LEVEL = 1.6 newdate = 12/29/16 REPORTING LEVEL = 1.6 newdate = 12/29/16 REPORTING LEVEL = 1.6 newdate = 12/15/16 REPORTING LEVEL = 1.6 newdate = 12/15/16 REPORTING LEVEL = 1.6 newdate = 12/07/16 REPORTING LEVEL = 1.6 newdate = 12/07/16 REPORTING LEVEL = 1.6 newdate = 09/21/16 REPORTING LEVEL = 1.6 newdate = 09/21/16 REPORTING LEVEL = 1.6 newdate = 09/15/16 REPORTING LEVEL = 1.6 newdate = 09/15/16 REPORTING LEVEL = 1.6 newdate = 09/09/16 REPORTING LEVEL = 1.6 newdate = 09/09/16 REPORTING LEVEL = 1.6 newdate = 08/19/16 REPORTING LEVEL = 1.6 newdate = 08/19/16 REPORTING LEVEL = 1.6 newdate = 08/11/16 REPORTING LEVEL = 1.6 newdate = 08/11/16 REPORTING LEVEL = 1.6 newdate = 07/12/16 REPORTING LEVEL = 1.6 newdate = 07/12/16 REPORTING LEVEL = 1.6 newdate = 06/24/16 REPORTING LEVEL = 1.6 newdate = 06/24/16 REPORTING LEVEL = 1.6 newdate = 03/18/16 REPORTING LEVEL = 0.8 newdate = 03/18/16 REPORTING LEVEL = 0.8 newdate = 03/18/16 REPORTING LEVEL = 0.8 newdate = 03/18/16 REPORTING LEVEL = 0.8 newdate = 03/07/16 REPORTING LEVEL = 0.8 newdate = 03/07/16 REPORTING LEVEL = 0.8 newdate = 03/07/16 REPORTING LEVEL = 0.8 Y = 0
The SGPlot Procedure

False Positive & Negative Listing for NORETHINDRONE

Status Lab ID Spike Mix Reporting Level Analysis Date Result Conc. Expected Conc.
False Negative 20160070058 ChemService 4073900: 30 µl & Abs 041515: 30 µl 0.8 03/07/16 < 0.8 1.204421
  20160280054 Abs 041515: 50 µl & ERA 0601-15-04: 50 µl 0.8 03/07/16 < 0.8 2.007368
  20160560045 Crescent 04EE007: 30 µl & Spex Organics EN150501025: 30 µl 0.8 03/18/16 < 0.8 1.2
  20160630047 Spex Organics EN150501025: 30 µl & Supelco LC13547: 30 µl 0.8 03/18/16 < 0.8 1.2
  20161400193 ChemService 5016100: 50 µl & Spex Organics TS160420010: 50 µl 1.6 08/11/16 < 3 3.357895
  20161820010 ChemService 5016200: 30 µl & Supelco LC20140V: 30 µl 1.6 09/09/16 < 1.6 2.021053
  20161960002 Supelco LC20140V: 30 µl & Spex Organics EN160621015: 30 µl 1.6 09/15/16 < 1.6 2.021053
  20170740061 Abs 061416H: 80 µl & ChemService 5016100: 80 µl 1.6 06/30/17 < 4.6 5.372632
  20171510081 Supelco LC20140V: 30 µl & ChemService 5016200: 30 µl 1.6 07/26/17 < 2 2.021053
  20171790208 ChemService 5016100: 50 µl & Abs 052616: 50 µl 1.6 08/30/17 < 3.3 3.357895
  20171870124 Supelco LC20140V: 50 µl & ChemService 5016200: 50 µl 1.6 09/28/17 < 1.6 3.368421

Updated 03/28/2018

back to table
Organic Blind Sample Program
False Positives & False Negatives
PROGESTERONE
Method: 4434 Testid: 64543GM005
Link to Individual Chart

newdate = 09/28/17 falseneg = -0.01 newdate = 07/28/17 falseneg = -0.01 newdate = 07/25/17 falseneg = -0.01 newdate = 07/13/17 falseneg = -0.01 newdate = 06/02/17 falseneg = -0.01 newdate = 09/09/16 falseneg = -0.01 newdate = 03/18/16 falseneg = -0.01 newdate = 03/18/16 falseneg = -0.01 newdate = 12/13/17 CENC_VAL = 75.000 newdate = 12/13/17 CENC_VAL = 8.100 newdate = 12/11/17 CENC_VAL = 49.000 newdate = 12/11/17 CENC_VAL = 45.000 newdate = 12/05/17 CENC_VAL = 66.300 newdate = 12/04/17 CENC_VAL = 8.100 newdate = 11/21/17 CENC_VAL = 10.500 newdate = 09/05/17 CENC_VAL = 10.800 newdate = 07/26/17 CENC_VAL = 7.900 newdate = 07/25/17 CENC_VAL = 13.300 newdate = 06/30/17 CENC_VAL = 41.500 newdate = 06/30/17 CENC_VAL = 14.100 newdate = 06/02/17 CENC_VAL = 15.500 newdate = 03/15/17 CENC_VAL = 7.800 newdate = 02/24/17 CENC_VAL = 12.600 newdate = 01/13/17 CENC_VAL = 9.500 newdate = 12/15/16 CENC_VAL = 13.400 newdate = 12/05/16 CENC_VAL = 8.400 newdate = 09/21/16 CENC_VAL = 7.300 newdate = 09/16/16 CENC_VAL = 8.900 newdate = 08/31/16 CENC_VAL = 19.300 newdate = 07/12/16 CENC_VAL = 7.200 newdate = 06/24/16 CENC_VAL = 6.700 newdate = 03/07/16 CENC_VAL = 12.300 newdate = 12/13/17 REPORTING LEVEL = 12 newdate = 12/13/17 REPORTING LEVEL = 12 newdate = 12/13/17 REPORTING LEVEL = 12 newdate = 12/11/17 REPORTING LEVEL = 12 newdate = 12/11/17 REPORTING LEVEL = 12 newdate = 12/11/17 REPORTING LEVEL = 12 newdate = 12/11/17 REPORTING LEVEL = 12 newdate = 12/05/17 REPORTING LEVEL = 12 newdate = 12/05/17 REPORTING LEVEL = 12 newdate = 12/04/17 REPORTING LEVEL = 12 newdate = 12/04/17 REPORTING LEVEL = 12 newdate = 11/21/17 REPORTING LEVEL = 12 newdate = 11/21/17 REPORTING LEVEL = 12 newdate = 09/28/17 REPORTING LEVEL = 12 newdate = 09/28/17 REPORTING LEVEL = 12 newdate = 09/05/17 REPORTING LEVEL = 12 newdate = 09/05/17 REPORTING LEVEL = 12 newdate = 07/28/17 REPORTING LEVEL = 12 newdate = 07/28/17 REPORTING LEVEL = 12 newdate = 07/26/17 REPORTING LEVEL = 12 newdate = 07/26/17 REPORTING LEVEL = 12 newdate = 07/25/17 REPORTING LEVEL = 12 newdate = 07/25/17 REPORTING LEVEL = 12 newdate = 07/25/17 REPORTING LEVEL = 12 newdate = 07/25/17 REPORTING LEVEL = 12 newdate = 07/13/17 REPORTING LEVEL = 12 newdate = 07/13/17 REPORTING LEVEL = 12 newdate = 06/30/17 REPORTING LEVEL = 12 newdate = 06/30/17 REPORTING LEVEL = 12 newdate = 06/30/17 REPORTING LEVEL = 12 newdate = 06/30/17 REPORTING LEVEL = 12 newdate = 06/02/17 REPORTING LEVEL = 12 newdate = 06/02/17 REPORTING LEVEL = 12 newdate = 06/02/17 REPORTING LEVEL = 12 newdate = 06/02/17 REPORTING LEVEL = 12 newdate = 03/15/17 REPORTING LEVEL = 12 newdate = 03/15/17 REPORTING LEVEL = 12 newdate = 02/24/17 REPORTING LEVEL = 12 newdate = 02/24/17 REPORTING LEVEL = 12 newdate = 01/13/17 REPORTING LEVEL = 12 newdate = 01/13/17 REPORTING LEVEL = 12 newdate = 12/15/16 REPORTING LEVEL = 12 newdate = 12/15/16 REPORTING LEVEL = 12 newdate = 12/07/16 REPORTING LEVEL = 12 newdate = 12/07/16 REPORTING LEVEL = 12 newdate = 12/05/16 REPORTING LEVEL = 12 newdate = 12/05/16 REPORTING LEVEL = 12 newdate = 09/21/16 REPORTING LEVEL = 12 newdate = 09/21/16 REPORTING LEVEL = 12 newdate = 09/16/16 REPORTING LEVEL = 12 newdate = 09/16/16 REPORTING LEVEL = 12 newdate = 09/09/16 REPORTING LEVEL = 12 newdate = 09/09/16 REPORTING LEVEL = 12 newdate = 08/31/16 REPORTING LEVEL = 12 newdate = 08/31/16 REPORTING LEVEL = 12 newdate = 07/12/16 REPORTING LEVEL = 12 newdate = 07/12/16 REPORTING LEVEL = 12 newdate = 06/24/16 REPORTING LEVEL = 12 newdate = 06/24/16 REPORTING LEVEL = 12 newdate = 03/18/16 REPORTING LEVEL = 8 newdate = 03/18/16 REPORTING LEVEL = 8 newdate = 03/18/16 REPORTING LEVEL = 8 newdate = 03/18/16 REPORTING LEVEL = 8 newdate = 03/07/16 REPORTING LEVEL = 8 Y = 0
The SGPlot Procedure

False Positive & Negative Listing for PROGESTERONE

Status Lab ID Spike Mix Reporting Level Analysis Date Result Conc. Expected Conc.
False Negative 20160430110 Supelco LC13547: 30 µl & ChemService 4073900: 30 µl 8 03/18/16 < 8 12
  20160630047 Spex Organics EN150501025: 30 µl & Supelco LC13547: 30 µl 8 03/18/16 < 8 12
  20161820010 ChemService 5016200: 30 µl & Supelco LC20140V: 30 µl 12 09/09/16 < 12 20.23579
  20170320041 Abs 052616: 50 µl & Abs 061416H: 50 µl 12 06/02/17 < 13.8 33.68
  20171020122 Abs 052616: 50 µl & ChemService 5016200: 50 µl 12 07/13/17 < 12 33.72631
  20171230084 Spex Organics EN160621015: 30 µl & Abs 061416H: 30 µl 12 07/25/17 < 12 20.208
  20171580162 Spex Organics EN160621015: 50 µl & Abs 061416H: 50 µl 12 07/28/17 < 20 33.68
  20171870124 Supelco LC20140V: 50 µl & ChemService 5016200: 50 µl 12 09/28/17 < 13 33.72631

Updated 03/28/2018

back to table
Organic Blind Sample Program
False Positives & False Negatives
TESTOSTERONE
Method: 4434 Testid: 64545GM005
Link to Individual Chart

newdate = 12/13/17 falseneg = -0.01 newdate = 07/25/17 falseneg = -0.01 newdate = 03/07/16 falseneg = -0.01 newdate = 07/26/17 falsepos = 8.1 newdate = 07/13/17 falsepos = 7.8 newdate = 12/13/17 CENC_VAL = 17.100 newdate = 12/11/17 CENC_VAL = 5.500 newdate = 09/05/17 CENC_VAL = 4.300 newdate = 07/28/17 CENC_VAL = 5.400 newdate = 07/25/17 CENC_VAL = 5.100 newdate = 06/30/17 CENC_VAL = 10.500 newdate = 06/30/17 CENC_VAL = 6.400 newdate = 06/02/17 CENC_VAL = 5.300 newdate = 06/02/17 CENC_VAL = 6.500 newdate = 02/24/17 CENC_VAL = 3.900 newdate = 12/15/16 CENC_VAL = 5.500 newdate = 12/05/16 CENC_VAL = 4.000 newdate = 07/12/16 CENC_VAL = 3.300 newdate = 06/24/16 CENC_VAL = 3.000 newdate = 03/18/16 CENC_VAL = 2.340 newdate = 03/18/16 CENC_VAL = 2.030 newdate = 12/13/17 REPORTING LEVEL = 1.6 newdate = 12/13/17 REPORTING LEVEL = 1.6 newdate = 12/13/17 REPORTING LEVEL = 1.6 newdate = 12/11/17 REPORTING LEVEL = 1.6 newdate = 12/11/17 REPORTING LEVEL = 1.6 newdate = 09/05/17 REPORTING LEVEL = 1.6 newdate = 09/05/17 REPORTING LEVEL = 1.6 newdate = 07/28/17 REPORTING LEVEL = 1.6 newdate = 07/28/17 REPORTING LEVEL = 1.6 newdate = 07/26/17 REPORTING LEVEL = 1.6 newdate = 07/26/17 REPORTING LEVEL = 1.6 newdate = 07/25/17 REPORTING LEVEL = 1.6 newdate = 07/25/17 REPORTING LEVEL = 1.6 newdate = 07/25/17 REPORTING LEVEL = 1.6 newdate = 07/25/17 REPORTING LEVEL = 1.6 newdate = 07/13/17 REPORTING LEVEL = 1.6 newdate = 07/13/17 REPORTING LEVEL = 1.6 newdate = 06/30/17 REPORTING LEVEL = 1.6 newdate = 06/30/17 REPORTING LEVEL = 1.6 newdate = 06/30/17 REPORTING LEVEL = 1.6 newdate = 06/30/17 REPORTING LEVEL = 1.6 newdate = 06/02/17 REPORTING LEVEL = 1.6 newdate = 06/02/17 REPORTING LEVEL = 1.6 newdate = 06/02/17 REPORTING LEVEL = 1.6 newdate = 06/02/17 REPORTING LEVEL = 1.6 newdate = 02/24/17 REPORTING LEVEL = 1.6 newdate = 02/24/17 REPORTING LEVEL = 1.6 newdate = 12/15/16 REPORTING LEVEL = 1.6 newdate = 12/15/16 REPORTING LEVEL = 1.6 newdate = 12/07/16 REPORTING LEVEL = 1.6 newdate = 12/07/16 REPORTING LEVEL = 1.6 newdate = 12/05/16 REPORTING LEVEL = 1.6 newdate = 12/05/16 REPORTING LEVEL = 1.6 newdate = 07/12/16 REPORTING LEVEL = 1.6 newdate = 07/12/16 REPORTING LEVEL = 1.6 newdate = 06/24/16 REPORTING LEVEL = 1.6 newdate = 06/24/16 REPORTING LEVEL = 1.6 newdate = 03/18/16 REPORTING LEVEL = 1.6 newdate = 03/18/16 REPORTING LEVEL = 1.6 newdate = 03/18/16 REPORTING LEVEL = 1.6 newdate = 03/18/16 REPORTING LEVEL = 1.6 newdate = 03/07/16 REPORTING LEVEL = 1.6 Y = 0
The SGPlot Procedure

False Positive & Negative Listing for TESTOSTERONE

Status Lab ID Spike Mix Reporting Level Analysis Date Result Conc. Expected Conc.
False Negative 20160280054 Abs 041515: 50 µl & ERA 0601-15-04: 50 µl 1.6 03/07/16 < 2.2 4.052631
  20171230084 Spex Organics EN160621015: 30 µl & Abs 061416H: 30 µl 1.6 07/25/17 < 2.6 3.99221
  20172700085 ChemService 6494400: 10 µl & ChemService 6507500: 10 µl 1.6 12/13/17 < 2.3 3.2
False Positive 20171020122 Abs 052616: 50 µl & ChemService 5016200: 50 µl 1.6 07/13/17 7.8 0
  20171380004 ChemService 5016100: 80 µl & Abs 052616: 80 µl 1.6 07/26/17 8.1 0

Updated 03/28/2018

back to table
Organic Blind Sample Program
False Positives & False Negatives
TRANS-DIETHYLSTILBESTROL
Method: 4434 Testid: 64536GM005
Link to Individual Chart

newdate = 08/30/17 falseneg = -0.01 newdate = 07/25/17 falseneg = -0.01 newdate = 12/05/16 falseneg = -0.01 newdate = 09/16/16 falseneg = -0.01 newdate = 09/15/16 falseneg = -0.01 newdate = 06/24/16 falseneg = -0.01 newdate = 03/18/16 falseneg = -0.01 newdate = 12/13/17 CENC_VAL = 48.200 newdate = 12/13/17 CENC_VAL = 5.100 newdate = 12/11/17 CENC_VAL = 38.700 newdate = 12/11/17 CENC_VAL = 6.600 newdate = 12/05/17 CENC_VAL = 6.900 newdate = 12/04/17 CENC_VAL = 4.000 newdate = 11/21/17 CENC_VAL = 4.100 newdate = 09/05/17 CENC_VAL = 1.800 newdate = 08/30/17 CENC_VAL = 2.000 newdate = 07/28/17 CENC_VAL = 1.700 newdate = 07/26/17 CENC_VAL = 3.000 newdate = 07/25/17 CENC_VAL = 1.800 newdate = 07/13/17 CENC_VAL = 1.700 newdate = 06/02/17 CENC_VAL = 1.600 newdate = 06/02/17 CENC_VAL = 2.300 newdate = 03/15/17 CENC_VAL = 3.100 newdate = 02/01/17 CENC_VAL = 1.300 newdate = 01/13/17 CENC_VAL = 1.500 newdate = 12/29/16 CENC_VAL = 1.300 newdate = 08/31/16 CENC_VAL = 1888.000 newdate = 08/19/16 CENC_VAL = 1874.000 newdate = 08/11/16 CENC_VAL = 1592.000 newdate = 06/24/16 CENC_VAL = 1.400 newdate = 03/18/16 CENC_VAL = 1.030 newdate = 03/07/16 CENC_VAL = 0.940 newdate = 12/13/17 REPORTING LEVEL = 1.3 newdate = 12/13/17 REPORTING LEVEL = 1.3 newdate = 12/13/17 REPORTING LEVEL = 1.3 newdate = 12/11/17 REPORTING LEVEL = 1.3 newdate = 12/11/17 REPORTING LEVEL = 1.3 newdate = 12/11/17 REPORTING LEVEL = 1.3 newdate = 12/11/17 REPORTING LEVEL = 1.3 newdate = 12/05/17 REPORTING LEVEL = 1.3 newdate = 12/05/17 REPORTING LEVEL = 1.3 newdate = 12/04/17 REPORTING LEVEL = 1.3 newdate = 12/04/17 REPORTING LEVEL = 1.3 newdate = 11/21/17 REPORTING LEVEL = 1.3 newdate = 11/21/17 REPORTING LEVEL = 1.3 newdate = 09/05/17 REPORTING LEVEL = 1.3 newdate = 09/05/17 REPORTING LEVEL = 1.3 newdate = 08/30/17 REPORTING LEVEL = 1.3 newdate = 08/30/17 REPORTING LEVEL = 1.3 newdate = 08/30/17 REPORTING LEVEL = 1.3 newdate = 08/30/17 REPORTING LEVEL = 1.3 newdate = 07/28/17 REPORTING LEVEL = 1.3 newdate = 07/28/17 REPORTING LEVEL = 1.3 newdate = 07/26/17 REPORTING LEVEL = 1.3 newdate = 07/26/17 REPORTING LEVEL = 1.3 newdate = 07/25/17 REPORTING LEVEL = 1.3 newdate = 07/25/17 REPORTING LEVEL = 1.3 newdate = 07/25/17 REPORTING LEVEL = 1.3 newdate = 07/25/17 REPORTING LEVEL = 1.3 newdate = 07/13/17 REPORTING LEVEL = 1.3 newdate = 07/13/17 REPORTING LEVEL = 1.3 newdate = 06/02/17 REPORTING LEVEL = 1.3 newdate = 06/02/17 REPORTING LEVEL = 1.3 newdate = 06/02/17 REPORTING LEVEL = 1.3 newdate = 06/02/17 REPORTING LEVEL = 1.3 newdate = 03/15/17 REPORTING LEVEL = 1.3 newdate = 03/15/17 REPORTING LEVEL = 1.3 newdate = 02/01/17 REPORTING LEVEL = 1.3 newdate = 02/01/17 REPORTING LEVEL = 1.3 newdate = 01/13/17 REPORTING LEVEL = 1.3 newdate = 01/13/17 REPORTING LEVEL = 1.3 newdate = 12/29/16 REPORTING LEVEL = 1.3 newdate = 12/29/16 REPORTING LEVEL = 1.3 newdate = 12/07/16 REPORTING LEVEL = 1.3 newdate = 12/07/16 REPORTING LEVEL = 1.3 newdate = 12/05/16 REPORTING LEVEL = 1.3 newdate = 12/05/16 REPORTING LEVEL = 1.3 newdate = 09/16/16 REPORTING LEVEL = 1.3 newdate = 09/16/16 REPORTING LEVEL = 1.3 newdate = 09/15/16 REPORTING LEVEL = 1.3 newdate = 09/15/16 REPORTING LEVEL = 1.3 newdate = 08/31/16 REPORTING LEVEL = 1.3 newdate = 08/31/16 REPORTING LEVEL = 1.3 newdate = 08/19/16 REPORTING LEVEL = 1.3 newdate = 08/19/16 REPORTING LEVEL = 1.3 newdate = 08/11/16 REPORTING LEVEL = 1.3 newdate = 08/11/16 REPORTING LEVEL = 1.3 newdate = 06/24/16 REPORTING LEVEL = 1.3 newdate = 06/24/16 REPORTING LEVEL = 1.3 newdate = 06/24/16 REPORTING LEVEL = 1.3 newdate = 06/24/16 REPORTING LEVEL = 1.3 newdate = 03/18/16 REPORTING LEVEL = 0.8 newdate = 03/18/16 REPORTING LEVEL = 0.8 newdate = 03/18/16 REPORTING LEVEL = 0.8 newdate = 03/18/16 REPORTING LEVEL = 0.8 newdate = 03/07/16 REPORTING LEVEL = 0.8 Y = 0
The SGPlot Procedure

False Positive & Negative Listing for TRANS-DIETHYLSTILBESTROL

Status Lab ID Spike Mix Reporting Level Analysis Date Result Conc. Expected Conc.
False Negative 20160430110 Supelco LC13547: 30 µl & ChemService 4073900: 30 µl 0.8 03/18/16 < 0.81 1.2
  20160910145 Crescent 04EE007: 50 µl & Spex Organics EN150501025: 50 µl 1.3 06/24/16 < 1.3 2
  20161960002 Supelco LC20140V: 30 µl & Spex Organics EN160621015: 30 µl 1.3 09/15/16 < 1.4 1.976842
  20162020125 Spex Organics EN160621015: 30 µl & ChemService 5016200: 30 µl 1.3 09/16/16 < 1.3 1.976842
  20162300273 Abs 052616: 30 µl & Abs 061416H: 30 µl 1.3 12/05/16 < 1.3 2.034947
  20171230084 Spex Organics EN160621015: 30 µl & Abs 061416H: 30 µl 1.3 07/25/17 < 1.3 1.976842
  20171790208 ChemService 5016100: 50 µl & Abs 052616: 50 µl 1.3 08/30/17 < 1.3 3.391579

Updated 03/28/2018