| BQS Organic Blind Sample Program |
| False Positives & False Negatives |
| 11-KETOTESTOSTERONE |
| Schedule: 4434 Testid: 64527GM005 |
| Link to Individual Chart |
| BQS Organic Blind Sample Project |
| False Positive and Negative Report for |
| Schedule: 4434 |
| Analyte | TestIDCode | CASNumber | # Samples Spiked |
# False Negatives |
# Samples Not Spiked |
# False Positives |
|---|---|---|---|---|---|---|
| 11-KETOTESTOSTERONE | 64527GM005 | 564-35-2 | 17 | 2 | 95 | 1 |
| 17-ALPHA-ESTRADIOL | 64528GM005 | 57-91-0 | 54 | 1 | 58 | 0 |
| 17-ALPHA-ETHYNYLESTRADIOL | 64529GM005 | 57-63-6 | 54 | 3 | 58 | 0 |
| 17-BETA-ESTRADIOL | 64530GM005 | 50-28-2 | 54 | 0 | 58 | 1 |
| 3-BETA-COPROSTANOL | 64532GM005 | 360-68-9 | 49 | 0 | 52 | 6 |
| 4-ANDROSTENE-3,17-DIONE | 64533GM005 | 63-05-8 | 22 | 0 | 90 | 2 |
| BISPHENOL A | 67305GM005 | 80-05-7 | 34 | 0 | 70 | 0 |
| CHOLESTEROL | 64534GM005 | 57-88-5 | 49 | 0 | 52 | 6 |
| CIS-ANDROSTERONE | 64535GM005 | 53-41-8 | 42 | 1 | 70 | 0 |
| DIHYDROTESTOSTERONE | 64544GM005 | 521-18-6 | 27 | 0 | 85 | 0 |
| EPITESTOSTERONE | 64537GM005 | 481-30-1 | 40 | 0 | 72 | 2 |
| EQUILENIN | 64538GM005 | 517-09-9 | 42 | 3 | 41 | 4 |
| EQUILIN | 64539GM005 | 474-86-2 | 61 | 11 | 51 | 0 |
| ESTRIOL | 64540GM005 | 50-27-1 | 67 | 5 | 45 | 3 |
| ESTRONE | 64541GM005 | 53-16-7 | 59 | 1 | 53 | 0 |
| MESTRANOL | 64542GM005 | 72-33-3 | 59 | 3 | 53 | 0 |
| NORETHINDRONE | 64531GM005 | 68-22-4 | 54 | 5 | 58 | 0 |
| PROGESTERONE | 64543GM005 | 57-83-0 | 61 | 2 | 51 | 0 |
| TESTOSTERONE | 64545GM005 | 58-22-0 | 25 | 0 | 87 | 0 |
| TRANS-DIETHYLSTILBESTROL | 64536GM005 | 56-53-1 | 59 | 6 | 53 | 0 |
| BQS Organic Blind Sample Program |
| False Positives & False Negatives |
| 11-KETOTESTOSTERONE |
| Schedule: 4434 Testid: 64527GM005 |
| Link to Individual Chart |
| False Positive & Negative Listing for 11-KETOTESTOSTERONE |
| Status | Lab ID | Spike Mix | Reporting Level | Analysis Date | Result Conc. | Expected Conc. |
|---|---|---|---|---|---|---|
| False Negative | 20101130056 | Restek A070624: 20 µl | 2 | 06/30/10 | < 2 | 3.31675 |
| 20102030011 | Restek A070624: 20 µl | 2 | 10/25/10 | < 2 | 3.341688 | |
| False Positive | 20080870099 | Supelco LB51755: 50 µl | 2 | 12/02/08 | E 0.49 | 0 |
| Updated 06/06/2013 |
| BQS Organic Blind Sample Program |
| False Positives & False Negatives |
| 17-ALPHA-ESTRADIOL |
| Schedule: 4434 Testid: 64528GM005 |
| Link to Individual Chart |
| False Positive & Negative Listing for 17-ALPHA-ESTRADIOL |
| Status | Lab ID | Spike Mix | Reporting Level | Analysis Date | Result Conc. | Expected Conc. |
|---|---|---|---|---|---|---|
| False Negative | 20080940066 | Restek A055510: 50 µl | 0.8 | 12/02/08 | < 1.27 | 1.803969 |
| Updated 06/06/2013 |
| BQS Organic Blind Sample Program |
| False Positives & False Negatives |
| 17-ALPHA-ETHYNYLESTRADIOL |
| Schedule: 4434 Testid: 64529GM005 |
| Link to Individual Chart |
| False Positive & Negative Listing for 17-ALPHA-ETHYNYLESTRADIOL |
| Status | Lab ID | Spike Mix | Reporting Level | Analysis Date | Result Conc. | Expected Conc. |
|---|---|---|---|---|---|---|
| False Negative | 20080940066 | Restek A055510: 50 µl | 0.8 | 12/02/08 | < 1.02 | 1.904189 |
| 20091210007 | Ultra CE-2887: 25 µl | 0.8 | 06/15/09 | < 1 | 1.042318 | |
| 20123490149 | ERA 0507-12-04.1: 25 µl & Supelco LB92781: 25 µl | 0.8 | 02/08/13 | < 0.8 | 1.057895 |
| Updated 06/06/2013 |
| BQS Organic Blind Sample Program |
| False Positives & False Negatives |
| 17-BETA-ESTRADIOL |
| Schedule: 4434 Testid: 64530GM005 |
| Link to Individual Chart |
| False Positive & Negative Listing for 17-BETA-ESTRADIOL |
| Status | Lab ID | Spike Mix | Reporting Level | Analysis Date | Result Conc. | Expected Conc. |
|---|---|---|---|---|---|---|
| False Positive | 20090500155 | ERA 0813-08-07H: 25 µl | 0.8 | 03/16/09 | E 0.14 | 0 |
| Updated 06/06/2013 |
| BQS Organic Blind Sample Program |
| False Positives & False Negatives |
| 3-BETA-COPROSTANOL |
| Schedule: 4434 Testid: 64532GM005 |
| Link to Individual Chart |
| False Positive & Negative Listing for 3-BETA-COPROSTANOL |
| Status | Lab ID | Spike Mix | Reporting Level | Analysis Date | Result Conc. | Expected Conc. |
|---|---|---|---|---|---|---|
| False Positive | 20072910001 | Abs 083107H: 50 µl | 2000 | 01/16/08 | E 169 | 0 |
| 20073380127 | Supelco LB51755: 50 µl | 2000 | 08/20/08 | E 2207 | 0 | |
| 20080080064 | Abs 083107H: 50 µl | 2000 | 08/20/08 | . 12780 | 0 | |
| 20080640004 | Abs 083107H: 50 µl | 2000 | 12/02/08 | E 178 | 0 | |
| 20080870099 | Supelco LB51755: 50 µl | 2000 | 12/02/08 | E 328 | 0 | |
| 20082260239 | Supelco LB51755: 50 µl | 2000 | 11/10/08 | E 20200 | 0 |
| Updated 06/06/2013 |
| BQS Organic Blind Sample Program |
| False Positives & False Negatives |
| 4-ANDROSTENE-3,17-DIONE |
| Schedule: 4434 Testid: 64533GM005 |
| Link to Individual Chart |
| False Positive & Negative Listing for 4-ANDROSTENE-3,17-DIONE |
| Status | Lab ID | Spike Mix | Reporting Level | Analysis Date | Result Conc. | Expected Conc. |
|---|---|---|---|---|---|---|
| False Positive | 20090210034 | Abs 081908H: 25 µl | 0.8 | 03/10/09 | E 2.06 | 0 |
| 20090300004 | Ultra CE-2887: 25 µl | 0.8 | 03/10/09 | E 1.8 | 0 |
| Updated 06/06/2013 |
| BQS Organic Blind Sample Program |
| False Positives & False Negatives |
| CHOLESTEROL |
| Schedule: 4434 Testid: 64534GM005 |
| Link to Individual Chart |
| False Positive & Negative Listing for CHOLESTEROL |
| Status | Lab ID | Spike Mix | Reporting Level | Analysis Date | Result Conc. | Expected Conc. |
|---|---|---|---|---|---|---|
| False Positive | 20072910001 | Abs 083107H: 50 µl | 2000 | 01/16/08 | E 240 | 0 |
| 20080080064 | Abs 083107H: 50 µl | 2000 | 08/20/08 | . 12240 | 0 | |
| 20080640004 | Abs 083107H: 50 µl | 2000 | 12/02/08 | E 434 | 0 | |
| 20080650060 | Abs 083107H: 50 µl | 2000 | 03/25/09 | E 6660 | 0 | |
| 20080870099 | Supelco LB51755: 50 µl | 2000 | 12/02/08 | E 408 | 0 | |
| 20082260239 | Supelco LB51755: 50 µl | 2000 | 11/10/08 | E 23900 | 0 |
| Updated 06/06/2013 |
| BQS Organic Blind Sample Program |
| False Positives & False Negatives |
| CIS-ANDROSTERONE |
| Schedule: 4434 Testid: 64535GM005 |
| Link to Individual Chart |
| False Positive & Negative Listing for CIS-ANDROSTERONE |
| Status | Lab ID | Spike Mix | Reporting Level | Analysis Date | Result Conc. | Expected Conc. |
|---|---|---|---|---|---|---|
| False Negative | 20080940066 | Restek A055510: 50 µl | 0.8 | 12/02/08 | < 0.8 | 1.403087 |
| Updated 06/06/2013 |
| BQS Organic Blind Sample Program |
| False Positives & False Negatives |
| EPITESTOSTERONE |
| Schedule: 4434 Testid: 64537GM005 |
| Link to Individual Chart |
| False Positive & Negative Listing for EPITESTOSTERONE |
| Status | Lab ID | Spike Mix | Reporting Level | Analysis Date | Result Conc. | Expected Conc. |
|---|---|---|---|---|---|---|
| False Positive | 20080650061 | Supelco LB51755: 50 µl | 4 | 03/25/09 | E 1.4 | 0 |
| 20092820007 | Abs 083109H: 20 µl | 4 | 12/03/09 | E 0.27 | 0 |
| Updated 06/06/2013 |
| BQS Organic Blind Sample Program |
| False Positives & False Negatives |
| EQUILENIN |
| Schedule: 4434 Testid: 64538GM005 |
| Link to Individual Chart |
| False Positive & Negative Listing for EQUILENIN |
| Status | Lab ID | Spike Mix | Reporting Level | Analysis Date | Result Conc. | Expected Conc. |
|---|---|---|---|---|---|---|
| False Negative | 20081930023 | Abs 083107H: 50 µl | 2 | 10/24/08 | < 2 | 3.505417 |
| 20091340063 | Supelco LB60732: 25 µl | 2 | 06/15/09 | < 2 | 6.204756 | |
| 20101830112 | Supelco LB69645: 20 µl | 2 | 10/25/10 | < 2 | 4.578564 | |
| False Positive | 20121670019 | Abs 051512: 25 µl | 2 | 08/24/12 | . 1.71 | 0 |
| 20122430224 | ERA 0507-12-04.1: 25 µl & Abs 051512: 25 µl | 2 | 11/01/12 | . 1.84 | 0 | |
| 20122930150 | Spex Organics T1120525010: 50 µl & Supelco LB92781: 50 µl | 2 | 12/18/12 | . 3.21 | 0 | |
| 20123490149 | ERA 0507-12-04.1: 25 µl & Supelco LB92781: 25 µl | 2 | 02/08/13 | . 2.45 | 0 |
| Updated 06/06/2013 |
| BQS Organic Blind Sample Program |
| False Positives & False Negatives |
| EQUILIN |
| Schedule: 4434 Testid: 64539GM005 |
| Link to Individual Chart |
| False Positive & Negative Listing for EQUILIN |
| Status | Lab ID | Spike Mix | Reporting Level | Analysis Date | Result Conc. | Expected Conc. |
|---|---|---|---|---|---|---|
| False Negative | 20080650060 | Abs 083107H: 50 µl | 4 | 03/25/09 | < 4 | 5.490118 |
| 20081340107 | Supelco LB51755: 50 µl | 4 | 12/02/08 | < 4.47 | 5.997819 | |
| 20081930023 | Abs 083107H: 50 µl | 4 | 10/24/08 | < 4 | 5.842362 | |
| 20091340063 | Supelco LB60732: 25 µl | 4 | 06/15/09 | < 4 | 6.876939 | |
| 20091830173 | Supelco LB60732: 25 µl | 4 | 08/11/09 | < 4 | 6.862745 | |
| 20100920052 | Supelco LB69645: 20 µl | 4 | 07/01/10 | < 4 | 6.204757 | |
| 20102030011 | Restek A070624: 20 µl | 4 | 10/25/10 | < 4 | 6.265665 | |
| 20102180082 | Supelco LB69645: 20 µl | 4 | 10/19/10 | < 4 | 6.216329 | |
| 20110070106 | Spex Organics T1100629008: 25 µl | 4 | 03/10/11 | < 4 | 5.220297 | |
| 20110340010 | Abs 081810: 25 µl | 4 | 03/30/11 | < 5.72 | 6.730172 | |
| 20111950200 | Spex Organics T1100629008: 100 µl | 4 | 09/29/11 | < 13.4 | 21.05263 |
| Updated 06/06/2013 |
| BQS Organic Blind Sample Program |
| False Positives & False Negatives |
| ESTRIOL |
| Schedule: 4434 Testid: 64540GM005 |
| Link to Individual Chart |
| False Positive & Negative Listing for ESTRIOL |
| Status | Lab ID | Spike Mix | Reporting Level | Analysis Date | Result Conc. | Expected Conc. |
|---|---|---|---|---|---|---|
| False Negative | 20081930023 | Abs 083107H: 50 µl | 2 | 10/24/08 | < 0.8 | 2.124495 |
| 20091970068 | Abs 081908H: 25 µl | 2 | 08/11/09 | < 2 | 2.083767 | |
| 20101830112 | Supelco LB69645: 20 µl | 2 | 10/25/10 | < 2 | 3.787721 | |
| 20101900007 | Abs 083109H: 40 µl | 2 | 10/25/10 | < 2 | 2.543451 | |
| 20102030011 | Restek A070624: 20 µl | 2 | 10/25/10 | < 2 | 3.759399 | |
| False Positive | 20090430175 | Supelco LB60732: 25 µl | 2 | 03/16/09 | E 0.43 | 0 |
| 20090500155 | ERA 0813-08-07H: 25 µl | 2 | 03/16/09 | E 0.88 | 0 | |
| 20090710019 | Supelco LB60732: 25 µl | 2 | 05/01/09 | E 0.5 | 0 |
| Updated 06/06/2013 |
| BQS Organic Blind Sample Program |
| False Positives & False Negatives |
| ESTRONE |
| Schedule: 4434 Testid: 64541GM005 |
| Link to Individual Chart |
| False Positive & Negative Listing for ESTRONE |
| Status | Lab ID | Spike Mix | Reporting Level | Analysis Date | Result Conc. | Expected Conc. |
|---|---|---|---|---|---|---|
| False Negative | 20081930023 | Abs 083107H: 50 µl | 0.8 | 10/24/08 | < 0.8 | 3.611642 |
| Updated 06/06/2013 |
| BQS Organic Blind Sample Program |
| False Positives & False Negatives |
| MESTRANOL |
| Schedule: 4434 Testid: 64542GM005 |
| Link to Individual Chart |
| False Positive & Negative Listing for MESTRANOL |
| Status | Lab ID | Spike Mix | Reporting Level | Analysis Date | Result Conc. | Expected Conc. |
|---|---|---|---|---|---|---|
| False Negative | 20080650060 | Abs 083107H: 50 µl | 0.8 | 03/25/09 | < 0.8 | 1.297664 |
| 20080650061 | Supelco LB51755: 50 µl | 0.8 | 03/25/09 | < 0.8 | 1.292761 | |
| 20081930023 | Abs 083107H: 50 µl | 0.8 | 10/24/08 | < 0.8 | 1.380922 |
| Updated 06/06/2013 |
| BQS Organic Blind Sample Program |
| False Positives & False Negatives |
| NORETHINDRONE |
| Schedule: 4434 Testid: 64531GM005 |
| Link to Individual Chart |
| False Positive & Negative Listing for NORETHINDRONE |
| Status | Lab ID | Spike Mix | Reporting Level | Analysis Date | Result Conc. | Expected Conc. |
|---|---|---|---|---|---|---|
| False Negative | 20090210034 | Abs 081908H: 25 µl | 0.8 | 03/10/09 | < 0.8 | 1.092385 |
| 20090920070 | Abs 081908H: 25 µl | 0.8 | 05/01/09 | < 0.86 | 1.098786 | |
| 20101900007 | Abs 083109H: 40 µl | 0.8 | 10/25/10 | < 0.8 | 1.695634 | |
| 20112100009 | Supelco LB77167: 25 µl | 0.8 | 09/29/11 | < 0.8 | 1.578947 | |
| 20112310028 | Crescent 162776: 25 µl | 0.8 | 10/12/11 | < 0.91 | 1.578947 |
| Updated 06/06/2013 |
| BQS Organic Blind Sample Program |
| False Positives & False Negatives |
| PROGESTERONE |
| Schedule: 4434 Testid: 64543GM005 |
| Link to Individual Chart |
| False Positive & Negative Listing for PROGESTERONE |
| Status | Lab ID | Spike Mix | Reporting Level | Analysis Date | Result Conc. | Expected Conc. |
|---|---|---|---|---|---|---|
| False Negative | 20101830112 | Supelco LB69645: 20 µl | 8 | 10/25/10 | < 8 | 9.157127 |
| 20113340044 | Abs 081810: 25 µl | 8 | 01/27/12 | < 8 | 9.473684 |
| Updated 06/06/2013 |
| BQS Organic Blind Sample Program |
| False Positives & False Negatives |
| TRANS-DIETHYLSTILBESTROL |
| Schedule: 4434 Testid: 64536GM005 |
| Link to Individual Chart |
| False Positive & Negative Listing for TRANS-DIETHYLSTILBESTROL |
| Status | Lab ID | Spike Mix | Reporting Level | Analysis Date | Result Conc. | Expected Conc. |
|---|---|---|---|---|---|---|
| False Negative | 20073060025 | Abs 083107H: 50 µl | 0.8 | 06/09/08 | < 0.8 | 1.852309 |
| 20073190234 | Supelco LB51755: 50 µl | 0.8 | 08/14/08 | < 0.8 | 1.445087 | |
| 20080240001 | Supelco LB51755: 50 µl | 0.8 | 08/20/08 | < 0.8 | 1.431298 | |
| 20080640004 | Abs 083107H: 50 µl | 0.8 | 12/02/08 | < 0.8 | 1.486031 | |
| 20080870099 | Supelco LB51755: 50 µl | 0.8 | 12/02/08 | < 0.8 | 1.5 | |
| 20081930023 | Abs 083107H: 50 µl | 0.8 | 10/24/08 | < 0.8 | 1.593372 |
| Updated 06/06/2013 |