SAS Output

BQS Organic Blind Sample Project

False Positive and Negative Report for

Schedule: 1433

Analyte	TestIDCode	CASNumber	# Samples Spiked	# False Negatives	# Samples Not Spiked	# False Positives
1,4-DICHLOROBENZENE	34572GCM37	106-46-7	93	1	107	1
1-METHYLNAPHTHALENE	62054GCM37	90-12-0	93	1	107	1
2,6-DIMETHYLNAPHTHALENE	62055GCM37	581-42-0	93	0	107	0
2-METHYLNAPHTHALENE	62056GCM37	91-57-6	93	1	107	1
3-BETA-COPROSTANOL	62057GCM37	360-68-9	89	1	111	0
3-METHYL-1(H)-INDOLE (SKATOLE)	62058GCM37	83-34-1	92	2	108	8
3-TERT-BUTYL-4-HYDROXY ANISOLE (BHA)	62059GCM37	121-00-6	87	0	113	0
4-CUMYLPHENOL	62060GCM37	599-64-4	93	3	107	0
4-N-OCTYLPHENOL	62061GCM37	1806-26-4	91	0	109	0
4-TERT-OCTYLPHENOL	62062GCM37	140-66-9	90	0	110	2
5-METHYL-1H-BENZOTRIAZOLE	62063GCM37	136-85-6	86	3	114	1
ACETOPHENONE	62064GCM37	98-86-2	90	1	110	0
ACETYL HEXAMETHYL TETRAHYDRONAPHTHALENE (AHTN)	62065GCM37	21145-77-7	57	0	143	0
ANTHRACENE	34221GCM37	120-12-7	93	1	107	2
ANTHRAQUINONE	62066GCM37	84-65-1	91	0	109	1
BENZOPHENONE	62067GCM37	119-61-9	92	0	108	13
BENZO[A]PYRENE	34248GCM37	50-32-8	93	0	107	0
BETA-SITOSTEROL	62068GCM37	83-46-5	76	3	124	2
BETA-STIGMASTANOL	62086GCM37	19466-47-8	89	2	111	0
BISPHENOL A	62069GCM37	80-05-7	64	2	89	0
BROMACIL	04029GCM37	314-40-9	91	1	109	0
BROMOFORM	34288GCM37	75-25-2	92	1	108	0
CAFFEINE	50305GCM37	58-08-2	92	1	108	2
CAMPHOR	62070GCM37	76-22-2	94	0	106	4
CARBARYL	82680GCM37	63-25-2	91	4	109	8
CARBAZOLE	62071GCM37	86-74-8	93	1	107	1
CHLORPYRIFOS	38933GCM37	2921-88-2	91	0	109	0
CHOLESTEROL	62072GCM37	57-88-5	89	1	111	0
COTININE	62005GCM37	486-56-6	91	2	109	0
D-LIMONENE	62073GCM37	5989-27-5	91	4	109	0
DIAZINON	39572GCM37	333-41-5	91	6	109	0
FLUORANTHENE	34377GCM37	206-44-0	93	1	107	0
HEXAHYDROHEXAMETHYLCYCLOPENTABENZOPYRAN (HHCB)	62075GCM37	1222-05-5	68	0	132	1
INDOLE	62076GCM37	120-72-9	91	2	109	0
ISOBORNEOL	62077GCM37	124-76-5	90	1	110	0
ISOPHORONE	34409GCM37	78-59-1	92	1	108	7
ISOPROPYLBENZENE (CUMENE)	62078GCM37	98-82-8	91	0	109	0
ISOQUINOLINE	62079GCM37	119-65-3	88	4	112	1
MENTHOL	62080GCM37	89-78-1	90	0	110	0
METALAXYL	50359GCM37	57837-19-1	90	1	110	0
METHYL SALICYLATE	62081GCM37	119-36-8	92	1	108	0
METOLACHLOR	39415GCM37	51218-45-2	91	1	109	1
N,N-DIETHYL-META-TOLUAMIDE (DEET)	62082GCM37	134-62-3	89	1	111	0
NAPHTHALENE	34443GCM37	91-20-3	92	1	108	0
NONYLPHENOL, DIETHOXY- (TOTAL)	62083GCM37	26027-38-3	48	11	152	2
OCTYLPHENOL, DIETHOXY-	61705GCM37	000-03-10	57	1	143	8
OCTYLPHENOL, MONOETHOXY-	61706GCM37	000-03-11	31	0	169	35
P-CRESOL	62084GCM37	106-44-5	89	1	111	0
PARA-NONYLPHENOL (TOTAL)	62085GCM37	84852-15-3	79	5	121	26
PENTACHLOROPHENOL	34459GCM37	87-86-5	63	0	90	0
PHENANTHRENE	34462GCM37	85-01-8	92	1	108	1
PHENOL	34466GCM37	108-95-2	89	0	111	1
PROMETON	04037GCM37	1610-18-0	91	0	109	0
PYRENE	34470GCM37	129-00-0	93	1	107	0
TETRACHLOROETHYLENE	34476GCM37	127-18-4	89	2	111	0
TRI(2-BUTOXYETHYL)PHOSPHATE	62093GCM37	78-51-3	89	0	111	1
TRI(2-CHLOROETHYL)PHOSPHATE	62087GCM37	115-96-8	91	0	109	3
TRIBUTYL PHOSPHATE	62089GCM37	126-73-8	91	0	109	0
TRICLOSAN	62090GCM37	3380-34-5	92	0	108	0
TRIETHYL CITRATE (ETHYL CITRATE)	62091GCM37	77-93-0	86	0	114	0
TRIPHENYL PHOSPHATE	62092GCM37	115-86-6	91	0	109	6
TRIS(DICHLORISOPROPYL)PHOSPHATE	62088GCM37	13674-87-8	91	0	109	0

BQS Organic Blind Sample Program

False Positives & False Negatives

1,4-DICHLOROBENZENE

Schedule: 1433 Testid: 34572GCM37

Link to Individual Chart

False Positive & Negative Listing for 1,4-DICHLOROBENZENE

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20090210032	Protocol D1080815007: 40 µl	0.04	01/29/09	< 0.04	1.920433
False Positive	20093450030	Restek A070024: 10 µl	0.04	02/23/10	E 0.0052	0

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

1-METHYLNAPHTHALENE

Schedule: 1433 Testid: 62054GCM37

Link to Individual Chart

False Positive & Negative Listing for 1-METHYLNAPHTHALENE

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20090210032	Protocol D1080815007: 40 µl	0.04	01/29/09	< 0.04	0.3999167
False Positive	20093520065	ChemService 480-95B: 80 µl	0.022	02/23/10	E 0.011	0

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

2-METHYLNAPHTHALENE

Schedule: 1433 Testid: 62056GCM37

Link to Individual Chart

False Positive & Negative Listing for 2-METHYLNAPHTHALENE

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20090210032	Protocol D1080815007: 40 µl	0.04	01/29/09	< 0.04	0.6040408
False Positive	20070640058	Accu B6080007: 25 µl	0.08	03/12/07	E 0.0048	0

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

3-BETA-COPROSTANOL

Schedule: 1433 Testid: 62057GCM37

Link to Individual Chart

False Positive & Negative Listing for 3-BETA-COPROSTANOL

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20082210030	NWQL BNA2SP053B: 75 µl	1	09/17/08	< 1.2	2.356175

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

3-METHYL-1(H)-INDOLE (SKATOLE)

Schedule: 1433 Testid: 62058GCM37

Link to Individual Chart

False Positive & Negative Listing for 3-METHYL-1(H)-INDOLE (SKATOLE)

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20090210032	Protocol D1080815007: 40 µl	0.04	01/29/09	< 0.04	1.937096
	20123200135	Spex Organics T1120521009: 10 µl & Abs 051112: 10 µl	0.036	12/05/12	< 0.036	0.15
False Positive	20070320005	ERA 0714-06-03: 10 µl & Crescent 08FF020: 10 µl & Crescent 08FF021: 10 µl	0.08	03/13/07	E 0.0024	0
	20071500017	Protocol F1060727002: 10 µl & Crescent 08FF020: 10 µl & Crescent 08FF021: 10 µl	0.08	08/14/07	E 0.0012	0
	20071710024	ERA 0714-06-03: 25 µl & Crescent 08FF020: 25 µl & Crescent 08FF021: 25 µl	0.08	08/20/07	E 0.006	0
	20083260004	ERA 0804-08-02WW: 40 µl	0.04	01/28/09	E 0.014	0
	20083400002	Abs 080508WW: 20 µl	0.04	01/08/09	E 0.007	0
	20083530109	ERA 0804-08-02WW: 20 µl	0.04	03/05/09	E 0.011	0
	20090160002	Abs 080508WW: 20 µl	0.04	01/29/09	E 0.0058	0
	20090920065	ERA 0804-08-02WW: 20 µl	0.04	04/23/09	E 0.0057	0

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

4-CUMYLPHENOL

Schedule: 1433 Testid: 62060GCM37

Link to Individual Chart

False Positive & Negative Listing for 4-CUMYLPHENOL

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20083460140	Protocol D1080815007: 20 µl	0.1	01/28/09	< 0.1	1.611825
	20090210032	Protocol D1080815007: 40 µl	0.1	01/29/09	< 0.1	3.315976
	20123200135	Spex Organics T1120521009: 10 µl & Abs 051112: 10 µl	0.06	12/05/12	< 0.06	0.15

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

4-TERT-OCTYLPHENOL

Schedule: 1433 Testid: 62062GCM37

Link to Individual Chart

False Positive & Negative Listing for 4-TERT-OCTYLPHENOL

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Positive	20122370104	Spex Organics T1120521009: 20 µl & Accu 212051389: 20 µl	0.14	10/11/12	E 0.016	0
	20122640133	Crescent 05BB047: 50 µl & Accu 212051389: 50 µl	0.14	10/11/12	E 0.037	0

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

5-METHYL-1H-BENZOTRIAZOLE

Schedule: 1433 Testid: 62063GCM37

Link to Individual Chart

False Positive & Negative Listing for 5-METHYL-1H-BENZOTRIAZOLE

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20071220019	ERA 0714-06-03: 25 µl & Crescent 08FF020: 25 µl & Crescent 08FF021: 25 µl	1.8	05/22/07	< 1.8	1.961652
	20090210032	Protocol D1080815007: 40 µl	2	01/29/09	< 2	3.340971
	20102810021	Accu 210091144: 20 µl	1.2	12/15/10	< 1.2	4.012938
False Positive	20111050152	Spex Organics T1100706008: 80 µl	1.2	04/28/11	. 0.29	0

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

ACETOPHENONE

Schedule: 1433 Testid: 62064GCM37

Link to Individual Chart

False Positive & Negative Listing for ACETOPHENONE

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20081630014	NWQL BNA2SP053B: 75 µl	0.4	07/12/08	< 0.59	0.5988024

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

ANTHRACENE

Schedule: 1433 Testid: 34221GCM37

Link to Individual Chart

False Positive & Negative Listing for ANTHRACENE

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20090210032	Protocol D1080815007: 40 µl	0.04	01/29/09	< 0.04	1.153926
False Positive	20110770002	Ultra CG-2301: 20 µl	0.01	04/06/11	. 0.09	0
	20112170171	Ultra CG-2301: 50 µl	0.01	08/26/11	. 0.19	0

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

ANTHRAQUINONE

Schedule: 1433 Testid: 62066GCM37

Link to Individual Chart

False Positive & Negative Listing for ANTHRAQUINONE

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Positive	20091410002	Protocol D1080815007: 20 µl	0.16	07/22/09	E 0.02	0

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

BENZOPHENONE

Schedule: 1433 Testid: 62067GCM37

Link to Individual Chart

False Positive & Negative Listing for BENZOPHENONE

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
False Positive	20072290015	Restek A046567: 25 µl & Crescent 08FF022: 25 µl	0.12	10/23/07	E 0.0264
	20072350249	Supelco LB40674: 25 µl	0.12	11/05/07	E 0.017
	20072490006	Abs 091106ww: 25 µl & Crescent 08FF023: 25 µl	0.12	11/14/07	E 0.013
	20072560017	Restek A046567: 25 µl & Crescent 08FF022: 25 µl	0.12	11/21/07	E 0.0077
	20072770005	Restek A053259: 25 µl	0.12	11/21/07	E 0.0272
	20072900074	Restek A053259: 25 µl	0.12	12/20/07	E 0.0251
	20073060021	Restek A053259: 25 µl	0.12	01/11/08	E 0.033
	20073110111	Crescent 07GG011: 25 µl	0.12	01/11/08	E 0.0329
	20073380129	Restek A053259: 25 µl	0.12	01/23/08	E 0.0381
	20073510135	Restek A053259: 25 µl	0.12	02/01/08	E 0.0258
	20080150155	Restek A053259: 25 µl	0.12	02/27/08	E 0.0184
	20080640003	Crescent 07GG011: 25 µl	0.12	03/31/08	E 0.0241
	20080870097	Crescent 07GG011: 25 µl	0.12	04/09/08	E 0.0335

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

BETA-SITOSTEROL

Schedule: 1433 Testid: 62068GCM37

Link to Individual Chart

False Positive & Negative Listing for BETA-SITOSTEROL

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20081630014	NWQL BNA2SP053B: 75 µl	1.6	07/11/08	< 1.6	2.39521
	20081840003	Crescent 07GG011: 25 µl	1.6	08/02/08	< 1.88	2.766798
	20082210030	NWQL BNA2SP053B: 75 µl	1.6	09/17/08	< 1.6	2.356175
False Positive	20111330147	Restek A075799: 50 µl	4	06/08/11	E 1.4	0
	20120370004	Restek A075799: 50 µl	4	03/09/12	E 0.8	0

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

BETA-STIGMASTANOL

Schedule: 1433 Testid: 62086GCM37

Link to Individual Chart

False Positive & Negative Listing for BETA-STIGMASTANOL

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20081630014	NWQL BNA2SP053B: 75 µl	1.2	07/12/08	< 1.47	2.39521
	20082210030	NWQL BNA2SP053B: 75 µl	1.2	09/17/08	< 1.2	2.356175

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

BISPHENOL A

Schedule: 1433 Testid: 62069GCM37

Link to Individual Chart

False Positive & Negative Listing for BISPHENOL A

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20082210030	NWQL BNA2SP053B: 75 µl	0.4	09/17/08	< 0.4	0.5890438
	20103230119	Restek A075799: 20 µl	2	01/29/11	< 2	2.958012

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

BROMACIL

Schedule: 1433 Testid: 04029GCM37

Link to Individual Chart

False Positive & Negative Listing for BROMACIL

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20102810021	Accu 210091144: 20 µl	0.36	12/15/10	< 0.36	0.8033963

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

BROMOFORM

Schedule: 1433 Testid: 34288GCM37

Link to Individual Chart

False Positive & Negative Listing for BROMOFORM

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20090210032	Protocol D1080815007: 40 µl	0.1	01/29/09	< 0.1	5.715476

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

CAFFEINE

Schedule: 1433 Testid: 50305GCM37

Link to Individual Chart

False Positive & Negative Listing for CAFFEINE

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20090210032	Protocol D1080815007: 40 µl	0.1	01/29/09	< 0.1	5.898771
False Positive	20102160003	ChemService 480-95B: 20 µl	0.06	10/14/10	E 0.028	0
	20123350008	Supelco LB92784: 10 µl & Accu 212051389: 10 µl	0.06	01/23/13	. 0.01	0

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

CAMPHOR

Schedule: 1433 Testid: 62070GCM37

Link to Individual Chart

False Positive & Negative Listing for CAMPHOR

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
False Positive	20070380003	Restek A046567: 25 µl & Crescent 08FF022: 25 µl	0.1	03/13/07	E 0.0067
	20111680032	Spex Organics T1100706008: 80 µl	0.044	07/22/11	. 0.009
	20112590003	Spex Organics T1100706008: 50 µl	0.044	11/04/11	. 0.02
	20122930149	Abs 051112: 100 µl & Accu 212051389: 100 µl	0.044	12/05/12	. 0.063

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

CARBARYL

Schedule: 1433 Testid: 82680GCM37

Link to Individual Chart

False Positive & Negative Listing for CARBARYL

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20093170003	ChemService 480-95B: 40 µl	0.38	01/21/10	< 0.38	0.5136418
	20122370104	Spex Organics T1120521009: 20 µl & Accu 212051389: 20 µl	0.16	10/11/12	< 0.16	0.2
	20122640133	Crescent 05BB047: 50 µl & Accu 212051389: 50 µl	0.16	10/11/12	< 0.16	0.5
	20122930149	Abs 051112: 100 µl & Accu 212051389: 100 µl	0.16	12/05/12	< 0.16	1
False Positive	20083110004	ChemService 406-104C: 40 µl	1	11/14/08	E 0.28	0
	20091130128	ChemService 406-104C: 40 µl	1	05/12/09	E 0.24	0
	20103020151	Ultra CG-2301: 80 µl	0.16	12/16/10	E 0.074	0
	20111680032	Spex Organics T1100706008: 80 µl	0.16	07/22/11	E 0.05	0
	20112590003	Spex Organics T1100706008: 50 µl	0.16	11/04/11	E 0.027	0
	20112870076	Ultra CG-2301: 20 µl	0.16	11/08/11	E 0.014	0
	20113500020	Ultra CG-2301: 80 µl	0.16	02/16/12	E 0.069	0
	20120620014	Ultra CG-2301: 20 µl	0.16	04/11/12	E 0.031	0

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

CARBAZOLE

Schedule: 1433 Testid: 62071GCM37

Link to Individual Chart

False Positive & Negative Listing for CARBAZOLE

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20090210032	Protocol D1080815007: 40 µl	0.04	01/29/09	< 0.04	3.940845
False Positive	20093520065	ChemService 480-95B: 80 µl	0.03	02/23/10	E 0.012	0

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

CHOLESTEROL

Schedule: 1433 Testid: 62072GCM37

Link to Individual Chart

False Positive & Negative Listing for CHOLESTEROL

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20093380006	Crescent 08LL076: 20 µl	2	02/05/10	< 2	2.004065

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

COTININE

Schedule: 1433 Testid: 62005GCM37

Link to Individual Chart

False Positive & Negative Listing for COTININE

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20072200100	Protocol F1060727002: 10 µl & Crescent 08FF020: 10 µl & Crescent 08FF021: 10 µl	0.4	10/19/07	< 0.583	0.7052942
	20101410008	Crescent 08LL076: 40 µl	0.6	08/04/10	< 0.6	0.8929111

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

D-LIMONENE

Schedule: 1433 Testid: 62073GCM37

Link to Individual Chart

False Positive & Negative Listing for D-LIMONENE

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20090210032	Protocol D1080815007: 40 µl	0.14	01/29/09	< 0.14	0.1583004
	20092460252	Protocol D1080815007: 40 µl	0.08	10/22/09	< 0.14	0.1523351
	20103330009	Ultra CG-2301: 20 µl	0.08	12/09/10	< 0.08	0.1438989
	20123200135	Spex Organics T1120521009: 10 µl & Abs 051112: 10 µl	0.08	12/05/12	< 0.08	0.151

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

DIAZINON

Schedule: 1433 Testid: 39572GCM37

Link to Individual Chart

False Positive & Negative Listing for DIAZINON

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20083460140	Protocol D1080815007: 20 µl	0.08	01/28/09	< 0.08	1.117748
	20090210032	Protocol D1080815007: 40 µl	0.08	01/29/09	< 0.08	2.299521
	20090780143	Protocol D1080815007: 20 µl	0.08	04/02/09	< 0.08	1.112903
	20091410002	Protocol D1080815007: 20 µl	0.08	07/22/09	< 0.08	1.095238
	20092040204	Protocol D1080815007: 20 µl	0.08	08/27/09	< 0.08	1.08994
	20092460252	Protocol D1080815007: 40 µl	0.16	10/22/09	< 0.08	2.212868

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

FLUORANTHENE

Schedule: 1433 Testid: 34377GCM37

Link to Individual Chart

False Positive & Negative Listing for FLUORANTHENE

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20090210032	Protocol D1080815007: 40 µl	0.04	01/29/09	< 0.04	2.81608

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

HEXAHYDROHEXAMETHYLCYCLOPENTABENZOPYRAN (HHCB)

Schedule: 1433 Testid: 62075GCM37

Link to Individual Chart

False Positive & Negative Listing for HEXAHYDROHEXAMETHYLCYCLOPENTABENZOPYRAN (HHCB)

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Positive	20112870076	Ultra CG-2301: 20 µl	0.052	11/08/11	. 0.0056	0

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

INDOLE

Schedule: 1433 Testid: 62076GCM37

Link to Individual Chart

False Positive & Negative Listing for INDOLE

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20122930149	Abs 051112: 100 µl & Accu 212051389: 100 µl	0.08	12/05/12	< 0.08	5.01
	20123200135	Spex Organics T1120521009: 10 µl & Abs 051112: 10 µl	0.08	12/05/12	< 0.08	0.501

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

ISOBORNEOL

Schedule: 1433 Testid: 62077GCM37

Link to Individual Chart

False Positive & Negative Listing for ISOBORNEOL

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20090210032	Protocol D1080815007: 40 µl	0.18	01/29/09	< 0.18	0.1957925

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

ISOPHORONE

Schedule: 1433 Testid: 34409GCM37

Link to Individual Chart

False Positive & Negative Listing for ISOPHORONE

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20090210032	Protocol D1080815007: 40 µl	0.08	01/29/09	< 0.08	0.2624453
False Positive	20081150078	Crescent 07GG011: 25 µl	0.08	05/20/08	E 0.0193	0
	20081290007	Supelco LB50015: 25 µl	0.08	06/03/08	E 0.0113	0
	20081840003	Crescent 07GG011: 25 µl	0.08	08/02/08	E 0.0093	0
	20082350004	Supelco LB50015: 25 µl	0.08	09/24/08	E 0.0131	0
	20082480189	Crescent 07GG011: 25 µl	0.08	10/08/08	E 0.0149	0
	20083400002	Abs 080508WW: 20 µl	0.08	01/08/09	E 0.0076	0
	20090300002	Supelco LB60966: 20 µl	0.08	03/05/09	E 0.0051	0

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

ISOQUINOLINE

Schedule: 1433 Testid: 62079GCM37

Link to Individual Chart

False Positive & Negative Listing for ISOQUINOLINE

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20102880004	Spex Organics T1100706008: 20 µl	0.046	12/08/10	< 0.08	0.1956715
	20103330009	Ultra CG-2301: 20 µl	0.046	12/09/10	< 0.08	0.1925134
	20121810018	Spex Organics T1120521009: 20 µl & Supelco LB92784: 20 µl	0.046	08/08/12	< 0.046	0.2
	20121950065	Crescent 05BB047: 10 µl & Abs 051112: 10 µl	0.046	08/08/12	< 0.046	0.1
False Positive	20112220131	NWQL BNA2SP124B: 50 µl	0.046	08/26/11	. 0.012	0

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

METALAXYL

Schedule: 1433 Testid: 50359GCM37

Link to Individual Chart

False Positive & Negative Listing for METALAXYL

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20090210032	Protocol D1080815007: 40 µl	0.12	01/29/09	< 0.12	1.932931

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

METHYL SALICYLATE

Schedule: 1433 Testid: 62081GCM37

Link to Individual Chart

False Positive & Negative Listing for METHYL SALICYLATE

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20081750161	Supelco LB50015: 25 µl	0.1	08/07/08	< 0.1	2.196894

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

METOLACHLOR

Schedule: 1433 Testid: 39415GCM37

Link to Individual Chart

False Positive & Negative Listing for METOLACHLOR

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20090210032	Protocol D1080815007: 40 µl	0.08	01/29/09	< 0.08	5.490523
False Positive	20070260003	Accu B6080007: 50 µl	0.16	03/13/07	E 0.0368	0

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

N,N-DIETHYL-META-TOLUAMIDE (DEET)

Schedule: 1433 Testid: 62082GCM37

Link to Individual Chart

False Positive & Negative Listing for N,N-DIETHYL-META-TOLUAMIDE (DEET)

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20081750161	Supelco LB50015: 25 µl	0.1	08/07/08	< 0.1	1.034569

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

NAPHTHALENE

Schedule: 1433 Testid: 34443GCM37

Link to Individual Chart

False Positive & Negative Listing for NAPHTHALENE

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20090210032	Protocol D1080815007: 40 µl	0.04	01/29/09	< 0.04	2.849406

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

NONYLPHENOL, DIETHOXY- (TOTAL)

Schedule: 1433 Testid: 62083GCM37

Link to Individual Chart

False Positive & Negative Listing for NONYLPHENOL, DIETHOXY- (TOTAL)

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20070440039	Abs 091106ww: 25 µl & Crescent 08FF023: 25 µl	5	03/13/07	< 5	6.037699
	20071860015	Abs 091106ww: 25 µl & Crescent 08FF023: 25 µl	5	09/06/07	< 5	6.112105
	20073110111	Crescent 07GG011: 25 µl	5	01/11/08	< 5	6.671384
	20081500005	Crescent 07GG011: 25 µl	5	06/03/08	< 5	6.576981
	20082480189	Crescent 07GG011: 25 µl	5	10/08/08	< 5	6.59868
	20093380006	Crescent 08LL076: 20 µl	5	02/05/10	< 5	5.288618
	20101410008	Crescent 08LL076: 40 µl	5	08/04/10	< 5	10.46556
	20102390089	Crescent 08LL076: 40 µl	5	11/04/10	< 5	10.49194
	20122370104	Spex Organics T1120521009: 20 µl & Accu 212051389: 20 µl	5	10/11/12	< 5	5.5
	20122640133	Crescent 05BB047: 50 µl & Accu 212051389: 50 µl	5	10/11/12	< 5	13.75
	20122930149	Abs 051112: 100 µl & Accu 212051389: 100 µl	5	12/05/12	< 5	27.5
False Positive	20070240005	NWQL WWS1SP134A: 50 µl	5	02/13/07	E 3.5	0
	20070860099	NWQL WWS1SP134A: 75 µl	5	04/25/07	E 7.91	0

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

OCTYLPHENOL, DIETHOXY-

Schedule: 1433 Testid: 61705GCM37

Link to Individual Chart

False Positive & Negative Listing for OCTYLPHENOL, DIETHOXY-

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20071710024	ERA 0714-06-03: 25 µl & Crescent 08FF020: 25 µl & Crescent 08FF021: 25 µl	1	08/20/07	< 1	1.164404
False Positive	20071860015	Abs 091106ww: 25 µl & Crescent 08FF023: 25 µl	1	09/06/07	E 0.0393	0
	20092960004	Crescent 08LL076: 80 µl	1	01/20/10	E 1.7	0
	20101410008	Crescent 08LL076: 40 µl	1	08/04/10	E 0.6	0
	20102390089	Crescent 08LL076: 40 µl	1	11/04/10	E 0.5	0
	20122370104	Spex Organics T1120521009: 20 µl & Accu 212051389: 20 µl	1	10/11/12	E 0.74	0
	20122640133	Crescent 05BB047: 50 µl & Accu 212051389: 50 µl	1	10/11/12	E 2.1	0
	20122930149	Abs 051112: 100 µl & Accu 212051389: 100 µl	1	12/05/12	E 6.5	0
	20123350008	Supelco LB92784: 10 µl & Accu 212051389: 10 µl	1	01/23/13	E 0.38	0

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

OCTYLPHENOL, MONOETHOXY-

Schedule: 1433 Testid: 61706GCM37

Link to Individual Chart

False Positive & Negative Listing for OCTYLPHENOL, MONOETHOXY-

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
False Positive	20070320005	ERA 0714-06-03: 10 µl & Crescent 08FF020: 10 µl & Crescent 08FF021: 10 µl	1	03/13/07	E 0.344
	20070520015	Protocol F1060727002: 25 µl & Crescent 08FF020: 25 µl & Crescent 08FF021: 25 µl	1	03/12/07	E 0.575
	20070720045	ERA 0714-06-03: 25 µl & Crescent 08FF020: 25 µl & Crescent 08FF021: 25 µl	1	04/18/07	E 0.547
	20071010007	ERA 0714-06-03: 10 µl & Crescent 08FF020: 10 µl & Crescent 08FF021: 10 µl	1	05/01/07	E 0.256
	20071070100	Protocol F1060727002: 25 µl & Crescent 08FF020: 25 µl & Crescent 08FF021: 25 µl	1	05/01/07	E 0.728
	20071220019	ERA 0714-06-03: 25 µl & Crescent 08FF020: 25 µl & Crescent 08FF021: 25 µl	1	05/22/07	E 0.555
	20071500017	Protocol F1060727002: 10 µl & Crescent 08FF020: 10 µl & Crescent 08FF021: 10 µl	1	08/14/07	E 0.286
	20071710024	ERA 0714-06-03: 25 µl & Crescent 08FF020: 25 µl & Crescent 08FF021: 25 µl	1	08/20/07	E 0.684
	20071920023	ERA 0714-06-03: 10 µl & Crescent 08FF020: 10 µl & Crescent 08FF021: 10 µl	1	09/10/07	E 0.316
	20072070015	Protocol F1060727002: 25 µl & Crescent 08FF020: 25 µl & Crescent 08FF021: 25 µl	1	10/01/07	E 0.644
	20072200100	Protocol F1060727002: 10 µl & Crescent 08FF020: 10 µl & Crescent 08FF021: 10 µl	1	10/19/07	E 0.3
	20072290014	Protocol F1060727002: 25 µl & Crescent 08FF020: 25 µl & Crescent 08FF021: 25 µl	1	10/23/07	E 0.84
	20072490002	Protocol F1060727002: 25 µl & Crescent 08FF020: 25 µl & Crescent 08FF021: 25 µl	1	11/14/07	E 0.651
	20073110111	Crescent 07GG011: 25 µl	1	01/11/08	E 1.43
	20080640003	Crescent 07GG011: 25 µl	1	03/31/08	E 1.32
	20080870097	Crescent 07GG011: 25 µl	1	04/09/08	E 1.32
	20081150078	Crescent 07GG011: 25 µl	1	05/20/08	E 1.51
	20081500005	Crescent 07GG011: 25 µl	1	06/03/08	E 1.48
	20081840003	Crescent 07GG011: 25 µl	1	08/02/08	E 1.5
	20082480189	Crescent 07GG011: 25 µl	1	10/08/08	E 1.24
	20083440104	Crescent 08HH017: 40 µl	1	01/27/09	E 4
	20090580005	Crescent 08HH017: 20 µl	1	03/21/09	E 2.8
	20090640122	Crescent 08HH017: 20 µl	1	03/24/09	E 2.7
	20091320006	Crescent 08HH017: 20 µl	1	06/03/09	E 2.3
	20091880137	Crescent 08HH017: 20 µl	1	08/26/09	E 2.4
	20092400049	Crescent 08HH017: 40 µl	1	10/21/09	E 5
	20092960004	Crescent 08LL076: 80 µl	1	01/20/10	E 4.5
	20093380006	Crescent 08LL076: 20 µl	1	02/05/10	E 0.54
	20101410008	Crescent 08LL076: 40 µl	1	08/04/10	E 1.8
	20102390089	Crescent 08LL076: 40 µl	1	11/04/10	E 1.7
	20111330147	Restek A075799: 50 µl	1	06/08/11	E 0.03
	20122370104	Spex Organics T1120521009: 20 µl & Accu 212051389: 20 µl	1	10/11/12	E 0.92
	20122640133	Crescent 05BB047: 50 µl & Accu 212051389: 50 µl	1	10/11/12	E 2.5
	20122930149	Abs 051112: 100 µl & Accu 212051389: 100 µl	1	12/05/12	E 7.4
	20123350008	Supelco LB92784: 10 µl & Accu 212051389: 10 µl	1	01/23/13	E 0.44

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

P-CRESOL

Schedule: 1433 Testid: 62084GCM37

Link to Individual Chart

False Positive & Negative Listing for P-CRESOL

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20121810018	Spex Organics T1120521009: 20 µl & Supelco LB92784: 20 µl	0.08	08/08/12	< 0.1	0.10008

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

PARA-NONYLPHENOL (TOTAL)

Schedule: 1433 Testid: 62085GCM37

Link to Individual Chart

False Positive & Negative Listing for PARA-NONYLPHENOL (TOTAL)

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20093100004	Accu 209081217: 20 µl	2	01/20/10	< 2	2.010488
	20093380006	Crescent 08LL076: 20 µl	2	02/05/10	< 2	2.063008
	20101410008	Crescent 08LL076: 40 µl	2	08/04/10	< 2	4.082454
	20101480009	Accu 209081217: 20 µl	2	08/04/10	< 2	2.038114
	20122930149	Abs 051112: 100 µl & Accu 212051389: 100 µl	2	12/05/12	< 2	15.01
False Positive	20072070015	Protocol F1060727002: 25 µl & Crescent 08FF020: 25 µl & Crescent 08FF021: 25 µl	1	10/01/07	E 1.42	0
	20072140014	Supelco LB40674: 25 µl	1	10/01/07	E 1.84	0
	20072200100	Protocol F1060727002: 10 µl & Crescent 08FF020: 10 µl & Crescent 08FF021: 10 µl	1	10/19/07	E 0.899	0
	20072290014	Protocol F1060727002: 25 µl & Crescent 08FF020: 25 µl & Crescent 08FF021: 25 µl	1	10/23/07	E 1.67	0
	20072290015	Restek A046567: 25 µl & Crescent 08FF022: 25 µl	1	10/23/07	E 2.45	0
	20072350249	Supelco LB40674: 25 µl	1	11/05/07	E 1.88	0
	20072490002	Protocol F1060727002: 25 µl & Crescent 08FF020: 25 µl & Crescent 08FF021: 25 µl	1	11/14/07	E 1.6	0
	20072560017	Restek A046567: 25 µl & Crescent 08FF022: 25 µl	1	11/21/07	E 0.691	0
	20072770005	Restek A053259: 25 µl	1	11/21/07	E 1.76	0
	20072900074	Restek A053259: 25 µl	1	12/20/07	E 2.01	0
	20073060021	Restek A053259: 25 µl	1	01/11/08	E 2.02	0
	20073240139	Restek A053259: 25 µl	1	01/14/08	E 1.78	0
	20073380129	Restek A053259: 25 µl	1	01/23/08	E 1.93	0
	20073510135	Restek A053259: 25 µl	1	02/01/08	E 1.66	0
	20080150155	Restek A053259: 25 µl	1	02/27/08	E 1.4	0
	20080580077	Supelco LB50015: 25 µl	1	03/31/08	E 2.2	0
	20080800002	Supelco LB50015: 25 µl	1	04/09/08	E 1.76	0
	20080940060	Supelco LB50015: 25 µl	1	04/21/08	E 18.2	0
	20081290007	Supelco LB50015: 25 µl	1	06/03/08	E 15.4	0
	20081750161	Supelco LB50015: 25 µl	1	08/07/08	E 13.1	0
	20082040252	Supelco LB50015: 25 µl	1	09/10/08	E 13.2	0
	20082350004	Supelco LB50015: 25 µl	1	09/24/08	E 8.16	0
	20083110004	ChemService 406-104C: 40 µl	2	11/14/08	E 0.495	0
	20090500129	Abs 080508WW: 40 µl	2	03/21/09	E 0.58	0
	20090780143	Protocol D1080815007: 20 µl	2	04/02/09	E 0.45	0
	20090920065	ERA 0804-08-02WW: 20 µl	2	04/23/09	E 0.33	0

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

PHENANTHRENE

Schedule: 1433 Testid: 34462GCM37

Link to Individual Chart

False Positive & Negative Listing for PHENANTHRENE

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20090210032	Protocol D1080815007: 40 µl	0.04	01/29/09	< 0.04	2.349511
False Positive	20070520015	Protocol F1060727002: 25 µl & Crescent 08FF020: 25 µl & Crescent 08FF021: 25 µl	0.08	03/12/07	E 0.0061	0

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

PHENOL

Schedule: 1433 Testid: 34466GCM37

Link to Individual Chart

False Positive & Negative Listing for PHENOL

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Positive	20070320005	ERA 0714-06-03: 10 µl & Crescent 08FF020: 10 µl & Crescent 08FF021: 10 µl	0.4	03/13/07	E 0.352	0

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

PYRENE

Schedule: 1433 Testid: 34470GCM37

Link to Individual Chart

False Positive & Negative Listing for PYRENE

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20090210032	Protocol D1080815007: 40 µl	0.04	01/29/09	< 0.04	0.7748386

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

TETRACHLOROETHYLENE

Schedule: 1433 Testid: 34476GCM37

Link to Individual Chart

False Positive & Negative Listing for TETRACHLOROETHYLENE

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Negative	20090210032	Protocol D1080815007: 40 µl	0.12	01/29/09	< 0.12	4.374089
	20122790025	Crescent 05BB047: 100 µl & Supelco LB92784: 100 µl	0.12	12/06/12	< 0.12	1.004

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

TRI(2-BUTOXYETHYL)PHOSPHATE

Schedule: 1433 Testid: 62093GCM37

Link to Individual Chart

False Positive & Negative Listing for TRI(2-BUTOXYETHYL)PHOSPHATE

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.	Expected Conc.
False Positive	20100420054	NSI 083109-01WW: 80 µl	0.8	03/25/10	E 0.1	0

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

TRI(2-CHLOROETHYL)PHOSPHATE

Schedule: 1433 Testid: 62087GCM37

Link to Individual Chart

False Positive & Negative Listing for TRI(2-CHLOROETHYL)PHOSPHATE

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
False Positive	20072560017	Restek A046567: 25 µl & Crescent 08FF022: 25 µl	0.1	11/21/07	E 0.053
	20082480189	Crescent 07GG011: 25 µl	0.1	10/08/08	. 0.108
	20092960004	Crescent 08LL076: 80 µl	0.1	01/20/10	E 0.07

Updated 06/06/2013

BQS Organic Blind Sample Program

False Positives & False Negatives

TRIPHENYL PHOSPHATE

Schedule: 1433 Testid: 62092GCM37

Link to Individual Chart

False Positive & Negative Listing for TRIPHENYL PHOSPHATE

Status	Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
False Positive	20092820006	NSI 083109-01WW: 20 µl	0.12	11/04/09	E 0.011
	20093340133	NSI 083109-01WW: 20 µl	0.12	02/03/10	E 0.009
	20100420054	NSI 083109-01WW: 80 µl	0.12	03/25/10	E 0.025
	20100500004	NSI 083109-01WW: 40 µl	0.12	03/25/10	E 0.018
	20101550005	NSI 083109-01WW: 40 µl	0.12	06/29/10	E 0.014
	20102810021	Accu 210091144: 20 µl	0.12	12/15/10	E 0.006

Updated 06/06/2013