Organic Blind Sample Program
False Positives & False Negatives
D-LIMONENE
Method: 4433 Testid: 62819GCM99
Link to Individual Chart

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newdate = 01/11/18 falseneg = -0.01 newdate = 04/14/17 falseneg = -0.01 newdate = 09/28/16 falseneg = -0.01 newdate = 02/24/16 falseneg = -0.01 newdate = 03/13/18 CENC_VAL = 0.859 newdate = 11/27/17 CENC_VAL = 0.486 newdate = 10/26/17 CENC_VAL = 0.442 newdate = 09/27/17 CENC_VAL = 0.601 newdate = 09/26/17 CENC_VAL = 0.238 newdate = 08/16/17 CENC_VAL = 0.261 newdate = 06/30/17 CENC_VAL = 0.695 newdate = 06/29/17 CENC_VAL = 0.576 newdate = 06/29/17 CENC_VAL = 0.329 newdate = 05/03/17 CENC_VAL = 0.325 newdate = 04/12/17 CENC_VAL = 0.365 newdate = 04/11/17 CENC_VAL = 0.982 newdate = 04/11/17 CENC_VAL = 0.441 newdate = 01/06/17 CENC_VAL = 1.150 newdate = 01/06/17 CENC_VAL = 0.500 newdate = 01/05/17 CENC_VAL = 0.426 newdate = 12/07/16 CENC_VAL = 0.278 newdate = 12/06/16 CENC_VAL = 0.521 newdate = 12/06/16 CENC_VAL = 0.633 newdate = 12/05/16 CENC_VAL = 2.100 newdate = 10/06/16 CENC_VAL = 0.337 newdate = 09/27/16 CENC_VAL = 0.293 newdate = 08/25/16 CENC_VAL = 0.584 newdate = 08/24/16 CENC_VAL = 0.329 newdate = 08/09/16 CENC_VAL = 0.963 newdate = 08/03/16 CENC_VAL = 0.346 newdate = 07/14/16 CENC_VAL = 0.364 newdate = 06/16/16 CENC_VAL = 0.409 newdate = 06/13/16 CENC_VAL = 0.376 newdate = 05/03/16 CENC_VAL = 0.657 newdate = 04/15/16 CENC_VAL = 0.453 newdate = 02/25/16 CENC_VAL = 0.304 newdate = 03/13/18 REPORTING LEVEL = 0.16 newdate = 01/11/18 REPORTING LEVEL = 0.16 newdate = 01/11/18 REPORTING LEVEL = 0.16 newdate = 11/27/17 REPORTING LEVEL = 0.16 newdate = 11/27/17 REPORTING LEVEL = 0.16 newdate = 10/26/17 REPORTING LEVEL = 0.16 newdate = 10/26/17 REPORTING LEVEL = 0.16 newdate = 09/27/17 REPORTING LEVEL = 0.16 newdate = 09/27/17 REPORTING LEVEL = 0.16 newdate = 09/27/17 REPORTING LEVEL = 0.16 newdate = 09/27/17 REPORTING LEVEL = 0.16 newdate = 09/26/17 REPORTING LEVEL = 0.16 newdate = 09/26/17 REPORTING LEVEL = 0.16 newdate = 08/16/17 REPORTING LEVEL = 0.16 newdate = 08/16/17 REPORTING LEVEL = 0.16 newdate = 06/30/17 REPORTING LEVEL = 0.16 newdate = 06/30/17 REPORTING LEVEL = 0.16 newdate = 06/29/17 REPORTING LEVEL = 0.16 newdate = 06/29/17 REPORTING LEVEL = 0.16 newdate = 06/29/17 REPORTING LEVEL = 0.16 newdate = 06/29/17 REPORTING LEVEL = 0.16 newdate = 05/03/17 REPORTING LEVEL = 0.16 newdate = 05/03/17 REPORTING LEVEL = 0.16 newdate = 04/14/17 REPORTING LEVEL = 0.16 newdate = 04/14/17 REPORTING LEVEL = 0.16 newdate = 04/12/17 REPORTING LEVEL = 0.16 newdate = 04/12/17 REPORTING LEVEL = 0.16 newdate = 04/11/17 REPORTING LEVEL = 0.16 newdate = 04/11/17 REPORTING LEVEL = 0.16 newdate = 04/11/17 REPORTING LEVEL = 0.16 newdate = 04/11/17 REPORTING LEVEL = 0.16 newdate = 01/06/17 REPORTING LEVEL = 0.16 newdate = 01/06/17 REPORTING LEVEL = 0.16 newdate = 01/06/17 REPORTING LEVEL = 0.16 newdate = 01/06/17 REPORTING LEVEL = 0.16 newdate = 01/05/17 REPORTING LEVEL = 0.16 newdate = 01/05/17 REPORTING LEVEL = 0.16 newdate = 12/07/16 REPORTING LEVEL = 0.16 newdate = 12/07/16 REPORTING LEVEL = 0.16 newdate = 12/06/16 REPORTING LEVEL = 0.16 newdate = 12/06/16 REPORTING LEVEL = 0.16 newdate = 12/06/16 REPORTING LEVEL = 0.16 newdate = 12/06/16 REPORTING LEVEL = 0.16 newdate = 12/05/16 REPORTING LEVEL = 0.16 newdate = 12/05/16 REPORTING LEVEL = 0.16 newdate = 10/06/16 REPORTING LEVEL = 0.16 newdate = 10/06/16 REPORTING LEVEL = 0.16 newdate = 09/28/16 REPORTING LEVEL = 0.16 newdate = 09/28/16 REPORTING LEVEL = 0.16 newdate = 09/27/16 REPORTING LEVEL = 0.16 newdate = 09/27/16 REPORTING LEVEL = 0.16 newdate = 09/26/16 REPORTING LEVEL = 0.16 newdate = 09/26/16 REPORTING LEVEL = 0.16 newdate = 08/25/16 REPORTING LEVEL = 0.16 newdate = 08/25/16 REPORTING LEVEL = 0.16 newdate = 08/24/16 REPORTING LEVEL = 0.16 newdate = 08/24/16 REPORTING LEVEL = 0.16 newdate = 08/09/16 REPORTING LEVEL = 0.16 newdate = 08/09/16 REPORTING LEVEL = 0.16 newdate = 08/03/16 REPORTING LEVEL = 0.16 newdate = 08/03/16 REPORTING LEVEL = 0.16 newdate = 08/01/16 REPORTING LEVEL = 0.16 newdate = 08/01/16 REPORTING LEVEL = 0.16 newdate = 07/14/16 REPORTING LEVEL = 0.16 newdate = 07/14/16 REPORTING LEVEL = 0.16 newdate = 06/16/16 REPORTING LEVEL = 0.16 newdate = 06/16/16 REPORTING LEVEL = 0.16 newdate = 06/13/16 REPORTING LEVEL = 0.16 newdate = 06/13/16 REPORTING LEVEL = 0.16 newdate = 05/03/16 REPORTING LEVEL = 0.16 newdate = 05/03/16 REPORTING LEVEL = 0.16 newdate = 04/15/16 REPORTING LEVEL = 0.16 newdate = 04/15/16 REPORTING LEVEL = 0.16 newdate = 02/25/16 REPORTING LEVEL = 0.16 newdate = 02/25/16 REPORTING LEVEL = 0.16 newdate = 02/24/16 REPORTING LEVEL = 0.16
The SGPlot Procedure

Updated 07/31/2018

False Positive & Negative Listing for D-LIMONENE

Status Lab ID Spike Mix Reporting Level Analysis Date Result Conc. Expected Conc.
False Negative 20160140040 Spex Organics EN150529012: 80 µl & Crescent 04EE006: 80 µl 0.16 02/24/16 < 0.858 0.96
  20162580142 Supelco LC20139V: 80 µl & Abs 061716WW: 80 µl 0.16 09/28/16 < 0.566 0.8
  20170820001 Supelco LC20139V: 40 µl & ChemService 5016000: 40 µl 0.16 04/14/17 < 0.396 0.4
  20173610076 Abs 071317WWUF: 60 µl & Abs 071717WWUF: 60 µl 0.16 01/11/18 < 0.16 0.6402

Updated 07/31/2018