Organic Blind Sample Program
False Positives & False Negatives
DESMETHYLDILTIAZEM
Method: 2440 Testid: 67999LCM56
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 newdate = 02/07/17 
 falseneg = -0.01  newdate = 02/07/17 
 falseneg = -0.01  newdate = 04/09/16 
 falseneg = -0.01  newdate = 11/09/17 
 CENC_VAL = 218.000  newdate = 11/09/17 
 CENC_VAL = 68.500  newdate = 11/08/17 
 CENC_VAL = 60.700  newdate = 10/21/17 
 CENC_VAL = 131.000  newdate = 09/23/17 
 CENC_VAL = 64.300  newdate = 09/21/17 
 CENC_VAL = 16.300  newdate = 09/09/17 
 CENC_VAL = 391.000  newdate = 08/28/17 
 CENC_VAL = 180.000  newdate = 08/26/17 
 CENC_VAL = 155.000  newdate = 08/11/17 
 CENC_VAL = 200.000  newdate = 08/10/17 
 CENC_VAL = 19.000  newdate = 07/15/17 
 CENC_VAL = 70.000  newdate = 07/14/17 
 CENC_VAL = 12.400  newdate = 06/18/17 
 CENC_VAL = 70.000  newdate = 06/17/17 
 CENC_VAL = 25.800  newdate = 05/11/17 
 CENC_VAL = 23.500  newdate = 04/20/17 
 CENC_VAL = 70.000  newdate = 04/07/17 
 CENC_VAL = 12.300  newdate = 04/07/17 
 CENC_VAL = 16.900  newdate = 04/06/17 
 CENC_VAL = 15.200  newdate = 04/06/17 
 CENC_VAL = 18.400  newdate = 03/14/17 
 CENC_VAL = 6.000  newdate = 03/14/17 
 CENC_VAL = 200.000  newdate = 01/19/17 
 CENC_VAL = 15.500  newdate = 01/19/17 
 CENC_VAL = 19.800  newdate = 01/05/17 
 CENC_VAL = 70.000  newdate = 01/05/17 
 CENC_VAL = 70.000  newdate = 11/18/16 
 CENC_VAL = 24.100  newdate = 11/18/16 
 CENC_VAL = 20.400  newdate = 11/18/16 
 CENC_VAL = 70.000  newdate = 11/18/16 
 CENC_VAL = 70.000  newdate = 10/29/16 
 CENC_VAL = 14.700  newdate = 10/29/16 
 CENC_VAL = 15.200  newdate = 10/28/16 
 CENC_VAL = 19.400  newdate = 10/28/16 
 CENC_VAL = 17.400  newdate = 09/23/16 
 CENC_VAL = 15.500  newdate = 09/23/16 
 CENC_VAL = 15.500  newdate = 09/17/16 
 CENC_VAL = 11.700  newdate = 09/17/16 
 CENC_VAL = 15.100  newdate = 09/09/16 
 CENC_VAL = 21.700  newdate = 09/09/16 
 CENC_VAL = 26.200  newdate = 08/17/16 
 CENC_VAL = 80.000  newdate = 08/17/16 
 CENC_VAL = 80.000  newdate = 08/11/16 
 CENC_VAL = 10.300  newdate = 08/11/16 
 CENC_VAL = 13.000  newdate = 07/23/16 
 CENC_VAL = 40.600  newdate = 07/23/16 
 CENC_VAL = 33.100  newdate = 05/11/16 
 CENC_VAL = 6.530  newdate = 05/11/16 
 CENC_VAL = 5.710  newdate = 04/27/16 
 CENC_VAL = 15.400  newdate = 04/27/16 
 CENC_VAL = 11.600  newdate = 04/27/16 
 CENC_VAL = 11.500  newdate = 04/09/16 
 CENC_VAL = 9.260  newdate = 11/09/17 
 REPORTING LEVEL = 70  newdate = 11/09/17 
 REPORTING LEVEL = 70  newdate = 11/09/17 
 REPORTING LEVEL = 70  newdate = 11/08/17 
 REPORTING LEVEL = 70  newdate = 11/08/17 
 REPORTING LEVEL = 70  newdate = 10/21/17 
 REPORTING LEVEL = 70  newdate = 10/21/17 
 REPORTING LEVEL = 70  newdate = 09/23/17 
 REPORTING LEVEL = 70  newdate = 09/23/17 
 REPORTING LEVEL = 70  newdate = 09/21/17 
 REPORTING LEVEL = 70  newdate = 09/21/17 
 REPORTING LEVEL = 70  newdate = 09/09/17 
 REPORTING LEVEL = 70  newdate = 09/09/17 
 REPORTING LEVEL = 70  newdate = 08/28/17 
 REPORTING LEVEL = 70  newdate = 08/28/17 
 REPORTING LEVEL = 70  newdate = 08/26/17 
 REPORTING LEVEL = 70  newdate = 08/26/17 
 REPORTING LEVEL = 70  newdate = 08/11/17 
 REPORTING LEVEL = 70  newdate = 08/11/17 
 REPORTING LEVEL = 70  newdate = 08/10/17 
 REPORTING LEVEL = 70  newdate = 08/10/17 
 REPORTING LEVEL = 70  newdate = 07/15/17 
 REPORTING LEVEL = 70  newdate = 07/15/17 
 REPORTING LEVEL = 70  newdate = 07/14/17 
 REPORTING LEVEL = 70  newdate = 07/14/17 
 REPORTING LEVEL = 70  newdate = 06/18/17 
 REPORTING LEVEL = 70  newdate = 06/18/17 
 REPORTING LEVEL = 70  newdate = 06/17/17 
 REPORTING LEVEL = 70  newdate = 06/17/17 
 REPORTING LEVEL = 70  newdate = 05/11/17 
 REPORTING LEVEL = 70  newdate = 05/11/17 
 REPORTING LEVEL = 70  newdate = 04/20/17 
 REPORTING LEVEL = 70  newdate = 04/20/17 
 REPORTING LEVEL = 70  newdate = 04/07/17 
 REPORTING LEVEL = 70  newdate = 04/07/17 
 REPORTING LEVEL = 70  newdate = 04/07/17 
 REPORTING LEVEL = 70  newdate = 04/07/17 
 REPORTING LEVEL = 70  newdate = 04/06/17 
 REPORTING LEVEL = 70  newdate = 04/06/17 
 REPORTING LEVEL = 70  newdate = 04/06/17 
 REPORTING LEVEL = 70  newdate = 04/06/17 
 REPORTING LEVEL = 70  newdate = 03/14/17 
 REPORTING LEVEL = 70  newdate = 03/14/17 
 REPORTING LEVEL = 70  newdate = 03/14/17 
 REPORTING LEVEL = 70  newdate = 03/14/17 
 REPORTING LEVEL = 70  newdate = 02/07/17 
 REPORTING LEVEL = 70  newdate = 02/07/17 
 REPORTING LEVEL = 70  newdate = 02/07/17 
 REPORTING LEVEL = 70  newdate = 02/07/17 
 REPORTING LEVEL = 70  newdate = 01/19/17 
 REPORTING LEVEL = 70  newdate = 01/19/17 
 REPORTING LEVEL = 70  newdate = 01/19/17 
 REPORTING LEVEL = 70  newdate = 01/19/17 
 REPORTING LEVEL = 70  newdate = 01/05/17 
 REPORTING LEVEL = 70  newdate = 01/05/17 
 REPORTING LEVEL = 70  newdate = 01/05/17 
 REPORTING LEVEL = 70  newdate = 01/05/17 
 REPORTING LEVEL = 70  newdate = 11/18/16 
 REPORTING LEVEL = 70  newdate = 11/18/16 
 REPORTING LEVEL = 70  newdate = 11/18/16 
 REPORTING LEVEL = 70  newdate = 11/18/16 
 REPORTING LEVEL = 70  newdate = 11/18/16 
 REPORTING LEVEL = 70  newdate = 11/18/16 
 REPORTING LEVEL = 70  newdate = 11/18/16 
 REPORTING LEVEL = 70  newdate = 11/18/16 
 REPORTING LEVEL = 70  newdate = 10/29/16 
 REPORTING LEVEL = 70  newdate = 10/29/16 
 REPORTING LEVEL = 70  newdate = 10/29/16 
 REPORTING LEVEL = 70  newdate = 10/29/16 
 REPORTING LEVEL = 70  newdate = 10/28/16 
 REPORTING LEVEL = 70  newdate = 10/28/16 
 REPORTING LEVEL = 70  newdate = 10/28/16 
 REPORTING LEVEL = 70  newdate = 10/28/16 
 REPORTING LEVEL = 70  newdate = 09/23/16 
 REPORTING LEVEL = 12.4  newdate = 09/23/16 
 REPORTING LEVEL = 12.4  newdate = 09/23/16 
 REPORTING LEVEL = 12.4  newdate = 09/23/16 
 REPORTING LEVEL = 12.4  newdate = 09/17/16 
 REPORTING LEVEL = 12.4  newdate = 09/17/16 
 REPORTING LEVEL = 12.4  newdate = 09/17/16 
 REPORTING LEVEL = 12.4  newdate = 09/17/16 
 REPORTING LEVEL = 12.4  newdate = 09/09/16 
 REPORTING LEVEL = 12.4  newdate = 09/09/16 
 REPORTING LEVEL = 12.4  newdate = 09/09/16 
 REPORTING LEVEL = 12.4  newdate = 09/09/16 
 REPORTING LEVEL = 12.4  newdate = 08/17/16 
 REPORTING LEVEL = 12.4  newdate = 08/17/16 
 REPORTING LEVEL = 12.4  newdate = 08/17/16 
 REPORTING LEVEL = 12.4  newdate = 08/17/16 
 REPORTING LEVEL = 12.4  newdate = 08/11/16 
 REPORTING LEVEL = 12.4  newdate = 08/11/16 
 REPORTING LEVEL = 12.4  newdate = 08/11/16 
 REPORTING LEVEL = 12.4  newdate = 08/11/16 
 REPORTING LEVEL = 12.4  newdate = 07/23/16 
 REPORTING LEVEL = 12.4  newdate = 07/23/16 
 REPORTING LEVEL = 12.4  newdate = 07/23/16 
 REPORTING LEVEL = 12.4  newdate = 07/23/16 
 REPORTING LEVEL = 12.4  newdate = 05/11/16 
 REPORTING LEVEL = 12.4  newdate = 05/11/16 
 REPORTING LEVEL = 12.4  newdate = 05/11/16 
 REPORTING LEVEL = 12.4  newdate = 05/11/16 
 REPORTING LEVEL = 12.4  newdate = 04/27/16 
 REPORTING LEVEL = 12.4  newdate = 04/27/16 
 REPORTING LEVEL = 12.4  newdate = 04/27/16 
 REPORTING LEVEL = 12.4  newdate = 04/27/16 
 REPORTING LEVEL = 12.4  newdate = 04/27/16 
 REPORTING LEVEL = 12.4  newdate = 04/27/16 
 REPORTING LEVEL = 12.4  newdate = 04/09/16 
 REPORTING LEVEL = 12.4  newdate = 04/09/16 
 REPORTING LEVEL = 12.4  newdate = 04/09/16 
 REPORTING LEVEL = 12.4  Y = 0
The SGPlot Procedure

Updated 03/27/2018

False Positive & Negative Listing for DESMETHYLDILTIAZEM

Status Lab ID Spike Mix Reporting Level Analysis Date Result Conc. Expected Conc.
False Negative 20160840084 ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl 12.4 04/09/16 < 12.4 18.54
  20170320038 Abs 061416: 100 µl & ERA 04281603: 100 µl 70 02/07/17 < 70 77.60001
  20170320039 Abs 061416: 100 µl & ERA 04281603: 100 µl 70 02/07/17 < 70 77.60001

Updated 03/27/2018