Organic Blind Sample Program
False Positives & False Negatives
TIOTROPIUM
Method: 2440 Testid: 67508LCM56
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newdate = 11/09/17 falseneg = -0.01 newdate = 11/09/17 falseneg = -0.01 newdate = 10/21/17 falseneg = -0.01 newdate = 05/11/16 falseneg = -0.01 newdate = 05/11/16 falseneg = -0.01 newdate = 11/08/17 CENC_VAL = 125.000 newdate = 09/23/17 CENC_VAL = 132.000 newdate = 09/21/17 CENC_VAL = 1010.000 newdate = 09/09/17 CENC_VAL = 3260.000 newdate = 08/28/17 CENC_VAL = 1090.000 newdate = 08/26/17 CENC_VAL = 425.000 newdate = 08/11/17 CENC_VAL = 31.000 newdate = 07/15/17 CENC_VAL = 16.000 newdate = 06/17/17 CENC_VAL = 85.000 newdate = 06/08/17 CENC_VAL = 66.000 newdate = 02/07/17 CENC_VAL = 54.000 newdate = 02/07/17 CENC_VAL = 49.000 newdate = 01/19/17 CENC_VAL = 41.000 newdate = 01/19/17 CENC_VAL = 46.000 newdate = 10/29/16 CENC_VAL = 39.000 newdate = 10/29/16 CENC_VAL = 35.000 newdate = 09/10/16 CENC_VAL = 7.170 newdate = 09/10/16 CENC_VAL = 17.600 newdate = 09/09/16 CENC_VAL = 39.600 newdate = 09/09/16 CENC_VAL = 66.000 newdate = 08/16/16 CENC_VAL = 60.000 newdate = 08/16/16 CENC_VAL = 57.100 newdate = 08/11/16 CENC_VAL = 3.370 newdate = 08/11/16 CENC_VAL = 3.910 newdate = 07/22/16 CENC_VAL = 50.100 newdate = 07/22/16 CENC_VAL = 48.800 newdate = 04/09/16 CENC_VAL = 29.500 newdate = 04/09/16 CENC_VAL = 10.200 newdate = 04/09/16 CENC_VAL = 43.100 newdate = 11/09/17 REPORTING LEVEL = 200 newdate = 11/09/17 REPORTING LEVEL = 200 newdate = 11/09/17 REPORTING LEVEL = 200 newdate = 11/08/17 REPORTING LEVEL = 200 newdate = 11/08/17 REPORTING LEVEL = 200 newdate = 10/21/17 REPORTING LEVEL = 200 newdate = 10/21/17 REPORTING LEVEL = 200 newdate = 09/23/17 REPORTING LEVEL = 200 newdate = 09/23/17 REPORTING LEVEL = 200 newdate = 09/21/17 REPORTING LEVEL = 200 newdate = 09/21/17 REPORTING LEVEL = 200 newdate = 09/09/17 REPORTING LEVEL = 200 newdate = 09/09/17 REPORTING LEVEL = 200 newdate = 08/28/17 REPORTING LEVEL = 200 newdate = 08/28/17 REPORTING LEVEL = 200 newdate = 08/26/17 REPORTING LEVEL = 200 newdate = 08/26/17 REPORTING LEVEL = 200 newdate = 08/11/17 REPORTING LEVEL = 200 newdate = 08/11/17 REPORTING LEVEL = 200 newdate = 07/15/17 REPORTING LEVEL = 200 newdate = 07/15/17 REPORTING LEVEL = 200 newdate = 06/17/17 REPORTING LEVEL = 200 newdate = 06/17/17 REPORTING LEVEL = 200 newdate = 06/08/17 REPORTING LEVEL = 200 newdate = 06/08/17 REPORTING LEVEL = 200 newdate = 04/20/17 REPORTING LEVEL = 200 newdate = 04/20/17 REPORTING LEVEL = 200 newdate = 02/07/17 REPORTING LEVEL = 200 newdate = 02/07/17 REPORTING LEVEL = 200 newdate = 02/07/17 REPORTING LEVEL = 200 newdate = 02/07/17 REPORTING LEVEL = 200 newdate = 01/19/17 REPORTING LEVEL = 200 newdate = 01/19/17 REPORTING LEVEL = 200 newdate = 01/19/17 REPORTING LEVEL = 200 newdate = 01/19/17 REPORTING LEVEL = 200 newdate = 10/29/16 REPORTING LEVEL = 200 newdate = 10/29/16 REPORTING LEVEL = 200 newdate = 10/29/16 REPORTING LEVEL = 200 newdate = 10/29/16 REPORTING LEVEL = 200 newdate = 09/10/16 REPORTING LEVEL = 43.1 newdate = 09/10/16 REPORTING LEVEL = 43.1 newdate = 09/10/16 REPORTING LEVEL = 43.1 newdate = 09/10/16 REPORTING LEVEL = 43.1 newdate = 09/09/16 REPORTING LEVEL = 43.1 newdate = 09/09/16 REPORTING LEVEL = 43.1 newdate = 09/09/16 REPORTING LEVEL = 43.1 newdate = 09/09/16 REPORTING LEVEL = 43.1 newdate = 08/16/16 REPORTING LEVEL = 43.1 newdate = 08/16/16 REPORTING LEVEL = 43.1 newdate = 08/16/16 REPORTING LEVEL = 43.1 newdate = 08/16/16 REPORTING LEVEL = 43.1 newdate = 08/11/16 REPORTING LEVEL = 43.1 newdate = 08/11/16 REPORTING LEVEL = 43.1 newdate = 08/11/16 REPORTING LEVEL = 43.1 newdate = 08/11/16 REPORTING LEVEL = 43.1 newdate = 07/22/16 REPORTING LEVEL = 43.1 newdate = 07/22/16 REPORTING LEVEL = 43.1 newdate = 07/22/16 REPORTING LEVEL = 43.1 newdate = 07/22/16 REPORTING LEVEL = 43.1 newdate = 05/11/16 REPORTING LEVEL = 43.1 newdate = 05/11/16 REPORTING LEVEL = 43.1 newdate = 05/11/16 REPORTING LEVEL = 43.1 newdate = 05/11/16 REPORTING LEVEL = 43.1 newdate = 04/09/16 REPORTING LEVEL = 43.1 newdate = 04/09/16 REPORTING LEVEL = 43.1 newdate = 04/09/16 REPORTING LEVEL = 43.1 newdate = 04/09/16 REPORTING LEVEL = 43.1 newdate = 04/09/16 REPORTING LEVEL = 43.1 Y = 0
The SGPlot Procedure

Updated 03/27/2018

False Positive & Negative Listing for TIOTROPIUM

Status Lab ID Spike Mix Reporting Level Analysis Date Result Conc. Expected Conc.
False Negative 20161260153 Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl 43.1 05/11/16 < 43.1 64.88
  20161260154 Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl 43.1 05/11/16 < 43.1 64.88
  20172700086 ERA 06281702: 50 µl & ERA 06281703: 50 µl 200 10/21/17 < 200 1000
  20172980057 ERA 06281702: 20 µl & Abs 072517Pharm2: 20 µl 200 11/09/17 < 200 400
  20173060003 ERA 06281704: 50 µl & ERA 06281702: 50 µl 200 11/09/17 < 200 1000

Updated 03/27/2018