Organic Blind Sample Program
False Positives & False Negatives
FIPRONIL_SULFONE
Method: 2437 Testid: 66613LCM60
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 newdate = 05/27/17 
 falseneg = -0.01  newdate = 12/13/16 
 falseneg = -0.01  newdate = 08/05/16 
 falseneg = -0.01  newdate = 07/08/16 
 falseneg = -0.01  newdate = 02/02/16 
 falseneg = -0.01  newdate = 10/11/17 
 CENC_VAL = 11.200  newdate = 10/04/17 
 CENC_VAL = 27.200  newdate = 09/22/17 
 CENC_VAL = 8.800  newdate = 08/24/17 
 CENC_VAL = 30.800  newdate = 08/08/17 
 CENC_VAL = 12.100  newdate = 07/26/17 
 CENC_VAL = 11.200  newdate = 07/11/17 
 CENC_VAL = 12.600  newdate = 06/21/17 
 CENC_VAL = 23.400  newdate = 06/13/17 
 CENC_VAL = 17.000  newdate = 05/23/17 
 CENC_VAL = 3.000  newdate = 05/06/17 
 CENC_VAL = 10.500  newdate = 04/18/17 
 CENC_VAL = 17.700  newdate = 02/28/17 
 CENC_VAL = 20.200  newdate = 02/28/17 
 CENC_VAL = 21.300  newdate = 02/16/17 
 CENC_VAL = 17.300  newdate = 02/16/17 
 CENC_VAL = 30.000  newdate = 01/28/17 
 CENC_VAL = 15.400  newdate = 01/28/17 
 CENC_VAL = 25.300  newdate = 01/17/17 
 CENC_VAL = 12.900  newdate = 01/17/17 
 CENC_VAL = 22.000  newdate = 12/13/16 
 CENC_VAL = 14.100  newdate = 12/13/16 
 CENC_VAL = 11.200  newdate = 12/13/16 
 CENC_VAL = 7.600  newdate = 11/29/16 
 CENC_VAL = 10.100  newdate = 11/29/16 
 CENC_VAL = 9.700  newdate = 11/09/16 
 CENC_VAL = 9.500  newdate = 11/09/16 
 CENC_VAL = 10.200  newdate = 10/21/16 
 CENC_VAL = 13.200  newdate = 10/21/16 
 CENC_VAL = 12.400  newdate = 10/20/16 
 CENC_VAL = 4.700  newdate = 10/20/16 
 CENC_VAL = 4.100  newdate = 09/29/16 
 CENC_VAL = 28.800  newdate = 09/29/16 
 CENC_VAL = 30.300  newdate = 09/21/16 
 CENC_VAL = 9.200  newdate = 09/21/16 
 CENC_VAL = 9.400  newdate = 09/07/16 
 CENC_VAL = 10.100  newdate = 09/07/16 
 CENC_VAL = 8.200  newdate = 08/31/16 
 CENC_VAL = 10.700  newdate = 08/31/16 
 CENC_VAL = 10.400  newdate = 08/20/16 
 CENC_VAL = 16.000  newdate = 08/20/16 
 CENC_VAL = 19.800  newdate = 08/12/16 
 CENC_VAL = 4.900  newdate = 08/12/16 
 CENC_VAL = 3.100  newdate = 08/05/16 
 CENC_VAL = 5.700  newdate = 08/05/16 
 CENC_VAL = 3.900  newdate = 08/05/16 
 CENC_VAL = 4.500  newdate = 07/22/16 
 CENC_VAL = 2.530  newdate = 07/22/16 
 CENC_VAL = 4.880  newdate = 07/08/16 
 CENC_VAL = 3.000  newdate = 05/10/16 
 CENC_VAL = 13.200  newdate = 05/10/16 
 CENC_VAL = 13.400  newdate = 05/05/16 
 CENC_VAL = 11.600  newdate = 05/05/16 
 CENC_VAL = 12.100  newdate = 03/23/16 
 CENC_VAL = 6.000  newdate = 03/23/16 
 CENC_VAL = 6.300  newdate = 03/23/16 
 CENC_VAL = 7.200  newdate = 03/09/16 
 CENC_VAL = 13.900  newdate = 03/09/16 
 CENC_VAL = 15.300  newdate = 03/09/16 
 CENC_VAL = 13.800  newdate = 03/01/16 
 CENC_VAL = 7.600  newdate = 03/01/16 
 CENC_VAL = 8.400  newdate = 03/01/16 
 CENC_VAL = 7.600  newdate = 02/20/16 
 CENC_VAL = 5.500  newdate = 02/20/16 
 CENC_VAL = 5.800  newdate = 02/20/16 
 CENC_VAL = 6.200  newdate = 02/09/16 
 CENC_VAL = 7.100  newdate = 02/09/16 
 CENC_VAL = 6.800  newdate = 02/09/16 
 CENC_VAL = 7.200  newdate = 02/02/16 
 CENC_VAL = 9.500  newdate = 02/02/16 
 CENC_VAL = 10.100  newdate = 02/02/16 
 CENC_VAL = 9.700  newdate = 02/02/16 
 CENC_VAL = 5.300  newdate = 02/02/16 
 CENC_VAL = 5.300  newdate = 10/11/17 
 REPORTING LEVEL = 5.6  newdate = 10/04/17 
 REPORTING LEVEL = 5.6  newdate = 10/04/17 
 REPORTING LEVEL = 5.6  newdate = 09/22/17 
 REPORTING LEVEL = 5.6  newdate = 09/22/17 
 REPORTING LEVEL = 5.6  newdate = 08/24/17 
 REPORTING LEVEL = 5.6  newdate = 08/24/17 
 REPORTING LEVEL = 5.6  newdate = 08/08/17 
 REPORTING LEVEL = 5.6  newdate = 08/08/17 
 REPORTING LEVEL = 5.6  newdate = 07/26/17 
 REPORTING LEVEL = 5.6  newdate = 07/26/17 
 REPORTING LEVEL = 5.6  newdate = 07/11/17 
 REPORTING LEVEL = 5.6  newdate = 07/11/17 
 REPORTING LEVEL = 5.6  newdate = 06/21/17 
 REPORTING LEVEL = 5.6  newdate = 06/21/17 
 REPORTING LEVEL = 5.6  newdate = 06/13/17 
 REPORTING LEVEL = 5.6  newdate = 06/13/17 
 REPORTING LEVEL = 5.6  newdate = 05/27/17 
 REPORTING LEVEL = 5.6  newdate = 05/27/17 
 REPORTING LEVEL = 5.6  newdate = 05/23/17 
 REPORTING LEVEL = 5.6  newdate = 05/23/17 
 REPORTING LEVEL = 5.6  newdate = 05/06/17 
 REPORTING LEVEL = 5.6  newdate = 05/06/17 
 REPORTING LEVEL = 5.6  newdate = 04/18/17 
 REPORTING LEVEL = 5.6  newdate = 04/18/17 
 REPORTING LEVEL = 5.6  newdate = 02/28/17 
 REPORTING LEVEL = 5.6  newdate = 02/28/17 
 REPORTING LEVEL = 5.6  newdate = 02/28/17 
 REPORTING LEVEL = 5.6  newdate = 02/28/17 
 REPORTING LEVEL = 5.6  newdate = 02/16/17 
 REPORTING LEVEL = 5.6  newdate = 02/16/17 
 REPORTING LEVEL = 5.6  newdate = 02/16/17 
 REPORTING LEVEL = 5.6  newdate = 02/16/17 
 REPORTING LEVEL = 5.6  newdate = 01/28/17 
 REPORTING LEVEL = 5.6  newdate = 01/28/17 
 REPORTING LEVEL = 5.6  newdate = 01/28/17 
 REPORTING LEVEL = 5.6  newdate = 01/28/17 
 REPORTING LEVEL = 5.6  newdate = 01/17/17 
 REPORTING LEVEL = 5.6  newdate = 01/17/17 
 REPORTING LEVEL = 5.6  newdate = 01/17/17 
 REPORTING LEVEL = 5.6  newdate = 01/17/17 
 REPORTING LEVEL = 5.6  newdate = 12/13/16 
 REPORTING LEVEL = 5.6  newdate = 12/13/16 
 REPORTING LEVEL = 5.6  newdate = 12/13/16 
 REPORTING LEVEL = 5.6  newdate = 12/13/16 
 REPORTING LEVEL = 5.6  newdate = 12/13/16 
 REPORTING LEVEL = 5.6  newdate = 12/13/16 
 REPORTING LEVEL = 5.6  newdate = 12/13/16 
 REPORTING LEVEL = 5.6  newdate = 12/13/16 
 REPORTING LEVEL = 5.6  newdate = 11/29/16 
 REPORTING LEVEL = 5.6  newdate = 11/29/16 
 REPORTING LEVEL = 5.6  newdate = 11/29/16 
 REPORTING LEVEL = 5.6  newdate = 11/29/16 
 REPORTING LEVEL = 5.6  newdate = 11/09/16 
 REPORTING LEVEL = 5.6  newdate = 11/09/16 
 REPORTING LEVEL = 5.6  newdate = 11/09/16 
 REPORTING LEVEL = 5.6  newdate = 11/09/16 
 REPORTING LEVEL = 5.6  newdate = 10/21/16 
 REPORTING LEVEL = 5.6  newdate = 10/21/16 
 REPORTING LEVEL = 5.6  newdate = 10/21/16 
 REPORTING LEVEL = 5.6  newdate = 10/21/16 
 REPORTING LEVEL = 5.6  newdate = 10/20/16 
 REPORTING LEVEL = 5.6  newdate = 10/20/16 
 REPORTING LEVEL = 5.6  newdate = 10/20/16 
 REPORTING LEVEL = 5.6  newdate = 10/20/16 
 REPORTING LEVEL = 5.6  newdate = 09/29/16 
 REPORTING LEVEL = 5.6  newdate = 09/29/16 
 REPORTING LEVEL = 5.6  newdate = 09/29/16 
 REPORTING LEVEL = 5.6  newdate = 09/29/16 
 REPORTING LEVEL = 5.6  newdate = 09/21/16 
 REPORTING LEVEL = 5.6  newdate = 09/21/16 
 REPORTING LEVEL = 5.6  newdate = 09/21/16 
 REPORTING LEVEL = 5.6  newdate = 09/21/16 
 REPORTING LEVEL = 5.6  newdate = 09/07/16 
 REPORTING LEVEL = 5.6  newdate = 09/07/16 
 REPORTING LEVEL = 5.6  newdate = 09/07/16 
 REPORTING LEVEL = 5.6  newdate = 09/07/16 
 REPORTING LEVEL = 5.6  newdate = 08/31/16 
 REPORTING LEVEL = 5.6  newdate = 08/31/16 
 REPORTING LEVEL = 5.6  newdate = 08/31/16 
 REPORTING LEVEL = 5.6  newdate = 08/31/16 
 REPORTING LEVEL = 5.6  newdate = 08/20/16 
 REPORTING LEVEL = 5.6  newdate = 08/20/16 
 REPORTING LEVEL = 5.6  newdate = 08/20/16 
 REPORTING LEVEL = 5.6  newdate = 08/20/16 
 REPORTING LEVEL = 5.6  newdate = 08/12/16 
 REPORTING LEVEL = 5.6  newdate = 08/12/16 
 REPORTING LEVEL = 5.6  newdate = 08/12/16 
 REPORTING LEVEL = 5.6  newdate = 08/12/16 
 REPORTING LEVEL = 5.6  newdate = 08/05/16 
 REPORTING LEVEL = 5.6  newdate = 08/05/16 
 REPORTING LEVEL = 5.6  newdate = 08/05/16 
 REPORTING LEVEL = 5.6  newdate = 08/05/16 
 REPORTING LEVEL = 5.6  newdate = 08/05/16 
 REPORTING LEVEL = 5.6  newdate = 08/05/16 
 REPORTING LEVEL = 5.6  newdate = 08/05/16 
 REPORTING LEVEL = 5.6  newdate = 08/05/16 
 REPORTING LEVEL = 5.6  newdate = 07/22/16 
 REPORTING LEVEL = 5.6  newdate = 07/22/16 
 REPORTING LEVEL = 5.6  newdate = 07/22/16 
 REPORTING LEVEL = 5.6  newdate = 07/22/16 
 REPORTING LEVEL = 5.6  newdate = 07/08/16 
 REPORTING LEVEL = 5.6  newdate = 07/08/16 
 REPORTING LEVEL = 5.6  newdate = 07/08/16 
 REPORTING LEVEL = 5.6  newdate = 07/08/16 
 REPORTING LEVEL = 5.6  newdate = 05/10/16 
 REPORTING LEVEL = 5.6  newdate = 05/10/16 
 REPORTING LEVEL = 5.6  newdate = 05/10/16 
 REPORTING LEVEL = 5.6  newdate = 05/10/16 
 REPORTING LEVEL = 5.6  newdate = 05/05/16 
 REPORTING LEVEL = 5.6  newdate = 05/05/16 
 REPORTING LEVEL = 5.6  newdate = 05/05/16 
 REPORTING LEVEL = 5.6  newdate = 05/05/16 
 REPORTING LEVEL = 5.6  newdate = 03/23/16 
 REPORTING LEVEL = 5.6  newdate = 03/23/16 
 REPORTING LEVEL = 5.6  newdate = 03/23/16 
 REPORTING LEVEL = 5.6  newdate = 03/23/16 
 REPORTING LEVEL = 5.6  newdate = 03/23/16 
 REPORTING LEVEL = 5.6  newdate = 03/23/16 
 REPORTING LEVEL = 5.6  newdate = 03/09/16 
 REPORTING LEVEL = 5.6  newdate = 03/09/16 
 REPORTING LEVEL = 5.6  newdate = 03/09/16 
 REPORTING LEVEL = 5.6  newdate = 03/09/16 
 REPORTING LEVEL = 5.6  newdate = 03/09/16 
 REPORTING LEVEL = 5.6  newdate = 03/09/16 
 REPORTING LEVEL = 5.6  newdate = 03/01/16 
 REPORTING LEVEL = 5.6  newdate = 03/01/16 
 REPORTING LEVEL = 5.6  newdate = 03/01/16 
 REPORTING LEVEL = 5.6  newdate = 03/01/16 
 REPORTING LEVEL = 5.6  newdate = 03/01/16 
 REPORTING LEVEL = 5.6  newdate = 03/01/16 
 REPORTING LEVEL = 5.6  newdate = 02/20/16 
 REPORTING LEVEL = 5.6  newdate = 02/20/16 
 REPORTING LEVEL = 5.6  newdate = 02/20/16 
 REPORTING LEVEL = 5.6  newdate = 02/20/16 
 REPORTING LEVEL = 5.6  newdate = 02/20/16 
 REPORTING LEVEL = 5.6  newdate = 02/20/16 
 REPORTING LEVEL = 5.6  newdate = 02/09/16 
 REPORTING LEVEL = 5.6  newdate = 02/09/16 
 REPORTING LEVEL = 5.6  newdate = 02/09/16 
 REPORTING LEVEL = 5.6  newdate = 02/09/16 
 REPORTING LEVEL = 5.6  newdate = 02/09/16 
 REPORTING LEVEL = 5.6  newdate = 02/09/16 
 REPORTING LEVEL = 5.6  newdate = 02/02/16 
 REPORTING LEVEL = 5.6  newdate = 02/02/16 
 REPORTING LEVEL = 5.6  newdate = 02/02/16 
 REPORTING LEVEL = 5.6  newdate = 02/02/16 
 REPORTING LEVEL = 5.6  newdate = 02/02/16 
 REPORTING LEVEL = 5.6  newdate = 02/02/16 
 REPORTING LEVEL = 5.6  newdate = 02/02/16 
 REPORTING LEVEL = 5.6  newdate = 02/02/16 
 REPORTING LEVEL = 5.6  newdate = 02/02/16 
 REPORTING LEVEL = 5.6  newdate = 02/02/16 
 REPORTING LEVEL = 5.6  newdate = 02/02/16 
 REPORTING LEVEL = 5.6
The SGPlot Procedure

Updated 08/13/2018

False Positive & Negative Listing for FIPRONIL_SULFONE

Status Lab ID Spike Mix Reporting Level Analysis Date Result Conc. Expected Conc.
False Negative 20160210083 ChemService 4047000: 10 µl & ChemService 3880000: 10 µl & ChemService 3995200: 1 5.6 02/02/16 < 5.6 6
  20161740281 Spex Organics TS160511023: 40 µl & ChemService 5154100: 40 µl & ChemService 5154 5.6 07/08/16 < 5.6 10
  20161960006 Spex Organics TS160511023: 40 µl & ChemService 5154100: 40 µl & ChemService 5154 5.6 08/05/16 < 5.6 10
  20163420124 Abs 071816: 40 µl & Spex Organics TS160603008: 40 µl 5.6 12/13/16 < 5.6 10.04
  20171440225 Abs 071216: 40 µl & Abs 071816: 40 µl 5.6 05/27/17 < 5.6 10.04

Updated 08/13/2018