Organic Blind Sample Program
False Positives & False Negatives
FIPRONIL
Method: 2437 Testid: 66604LCM60
Link to Individual Chart

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 newdate = 07/26/17 
 falseneg = -0.01  newdate = 05/27/17 
 falseneg = -0.01  newdate = 12/13/16 
 falseneg = -0.01  newdate = 08/05/16 
 falseneg = -0.01  newdate = 06/27/17 
 falsepos = 1.45  newdate = 05/17/17 
 falsepos = 1.83  newdate = 10/11/17 
 CENC_VAL = 6.290  newdate = 10/04/17 
 CENC_VAL = 19.700  newdate = 09/22/17 
 CENC_VAL = 6.080  newdate = 08/24/17 
 CENC_VAL = 20.800  newdate = 08/08/17 
 CENC_VAL = 9.510  newdate = 07/11/17 
 CENC_VAL = 13.900  newdate = 06/21/17 
 CENC_VAL = 17.400  newdate = 06/13/17 
 CENC_VAL = 16.000  newdate = 05/23/17 
 CENC_VAL = 4.250  newdate = 05/06/17 
 CENC_VAL = 9.730  newdate = 04/18/17 
 CENC_VAL = 13.700  newdate = 02/28/17 
 CENC_VAL = 20.200  newdate = 02/28/17 
 CENC_VAL = 18.000  newdate = 02/16/17 
 CENC_VAL = 20.200  newdate = 02/16/17 
 CENC_VAL = 28.800  newdate = 01/28/17 
 CENC_VAL = 18.800  newdate = 01/28/17 
 CENC_VAL = 23.000  newdate = 01/17/17 
 CENC_VAL = 18.200  newdate = 01/17/17 
 CENC_VAL = 21.200  newdate = 12/13/16 
 CENC_VAL = 16.200  newdate = 12/13/16 
 CENC_VAL = 15.300  newdate = 12/13/16 
 CENC_VAL = 9.610  newdate = 11/29/16 
 CENC_VAL = 10.100  newdate = 11/29/16 
 CENC_VAL = 8.900  newdate = 11/09/16 
 CENC_VAL = 9.820  newdate = 11/09/16 
 CENC_VAL = 8.940  newdate = 10/21/16 
 CENC_VAL = 11.900  newdate = 10/21/16 
 CENC_VAL = 12.100  newdate = 10/20/16 
 CENC_VAL = 4.410  newdate = 10/20/16 
 CENC_VAL = 3.300  newdate = 09/29/16 
 CENC_VAL = 29.000  newdate = 09/29/16 
 CENC_VAL = 27.700  newdate = 09/21/16 
 CENC_VAL = 7.670  newdate = 09/21/16 
 CENC_VAL = 9.560  newdate = 09/07/16 
 CENC_VAL = 8.460  newdate = 09/07/16 
 CENC_VAL = 8.230  newdate = 08/31/16 
 CENC_VAL = 9.430  newdate = 08/31/16 
 CENC_VAL = 8.710  newdate = 08/20/16 
 CENC_VAL = 16.600  newdate = 08/20/16 
 CENC_VAL = 17.000  newdate = 08/12/16 
 CENC_VAL = 7.730  newdate = 08/12/16 
 CENC_VAL = 6.050  newdate = 08/05/16 
 CENC_VAL = 5.740  newdate = 08/05/16 
 CENC_VAL = 4.910  newdate = 08/05/16 
 CENC_VAL = 5.410  newdate = 07/22/16 
 CENC_VAL = 2.970  newdate = 07/22/16 
 CENC_VAL = 6.330  newdate = 07/08/16 
 CENC_VAL = 3.090  newdate = 07/08/16 
 CENC_VAL = 2.920  newdate = 05/10/16 
 CENC_VAL = 10.800  newdate = 05/10/16 
 CENC_VAL = 12.300  newdate = 03/23/16 
 CENC_VAL = 6.100  newdate = 03/23/16 
 CENC_VAL = 7.180  newdate = 03/23/16 
 CENC_VAL = 6.770  newdate = 03/16/16 
 CENC_VAL = 18.400  newdate = 03/16/16 
 CENC_VAL = 17.700  newdate = 03/16/16 
 CENC_VAL = 17.100  newdate = 03/01/16 
 CENC_VAL = 13.700  newdate = 03/01/16 
 CENC_VAL = 11.300  newdate = 03/01/16 
 CENC_VAL = 12.400  newdate = 03/01/16 
 CENC_VAL = 6.330  newdate = 03/01/16 
 CENC_VAL = 7.380  newdate = 03/01/16 
 CENC_VAL = 8.270  newdate = 02/09/16 
 CENC_VAL = 7.290  newdate = 02/09/16 
 CENC_VAL = 6.410  newdate = 02/09/16 
 CENC_VAL = 6.580  newdate = 02/09/16 
 CENC_VAL = 6.150  newdate = 02/09/16 
 CENC_VAL = 7.350  newdate = 02/09/16 
 CENC_VAL = 6.160  newdate = 02/02/16 
 CENC_VAL = 11.400  newdate = 02/02/16 
 CENC_VAL = 10.900  newdate = 02/02/16 
 CENC_VAL = 10.700  newdate = 01/27/16 
 CENC_VAL = 5.730  newdate = 01/27/16 
 CENC_VAL = 4.850  newdate = 01/27/16 
 CENC_VAL = 5.190  newdate = 10/11/17 
 REPORTING LEVEL = 4  newdate = 10/04/17 
 REPORTING LEVEL = 4  newdate = 10/04/17 
 REPORTING LEVEL = 4  newdate = 09/22/17 
 REPORTING LEVEL = 4  newdate = 09/22/17 
 REPORTING LEVEL = 4  newdate = 08/24/17 
 REPORTING LEVEL = 4  newdate = 08/24/17 
 REPORTING LEVEL = 4  newdate = 08/08/17 
 REPORTING LEVEL = 4  newdate = 08/08/17 
 REPORTING LEVEL = 4  newdate = 07/26/17 
 REPORTING LEVEL = 4  newdate = 07/26/17 
 REPORTING LEVEL = 4  newdate = 07/11/17 
 REPORTING LEVEL = 4  newdate = 07/11/17 
 REPORTING LEVEL = 4  newdate = 06/27/17 
 REPORTING LEVEL = 4  newdate = 06/27/17 
 REPORTING LEVEL = 4  newdate = 06/21/17 
 REPORTING LEVEL = 4  newdate = 06/21/17 
 REPORTING LEVEL = 4  newdate = 06/13/17 
 REPORTING LEVEL = 4  newdate = 06/13/17 
 REPORTING LEVEL = 4  newdate = 05/27/17 
 REPORTING LEVEL = 4  newdate = 05/27/17 
 REPORTING LEVEL = 4  newdate = 05/23/17 
 REPORTING LEVEL = 4  newdate = 05/23/17 
 REPORTING LEVEL = 4  newdate = 05/17/17 
 REPORTING LEVEL = 4  newdate = 05/17/17 
 REPORTING LEVEL = 4  newdate = 05/06/17 
 REPORTING LEVEL = 4  newdate = 05/06/17 
 REPORTING LEVEL = 4  newdate = 04/18/17 
 REPORTING LEVEL = 4  newdate = 04/18/17 
 REPORTING LEVEL = 4  newdate = 02/28/17 
 REPORTING LEVEL = 4  newdate = 02/28/17 
 REPORTING LEVEL = 4  newdate = 02/28/17 
 REPORTING LEVEL = 4  newdate = 02/28/17 
 REPORTING LEVEL = 4  newdate = 02/16/17 
 REPORTING LEVEL = 4  newdate = 02/16/17 
 REPORTING LEVEL = 4  newdate = 02/16/17 
 REPORTING LEVEL = 4  newdate = 02/16/17 
 REPORTING LEVEL = 4  newdate = 01/28/17 
 REPORTING LEVEL = 4  newdate = 01/28/17 
 REPORTING LEVEL = 4  newdate = 01/28/17 
 REPORTING LEVEL = 4  newdate = 01/28/17 
 REPORTING LEVEL = 4  newdate = 01/17/17 
 REPORTING LEVEL = 4  newdate = 01/17/17 
 REPORTING LEVEL = 4  newdate = 01/17/17 
 REPORTING LEVEL = 4  newdate = 01/17/17 
 REPORTING LEVEL = 4  newdate = 12/13/16 
 REPORTING LEVEL = 4  newdate = 12/13/16 
 REPORTING LEVEL = 4  newdate = 12/13/16 
 REPORTING LEVEL = 4  newdate = 12/13/16 
 REPORTING LEVEL = 4  newdate = 12/13/16 
 REPORTING LEVEL = 4  newdate = 12/13/16 
 REPORTING LEVEL = 4  newdate = 12/13/16 
 REPORTING LEVEL = 4  newdate = 12/13/16 
 REPORTING LEVEL = 4  newdate = 11/29/16 
 REPORTING LEVEL = 4  newdate = 11/29/16 
 REPORTING LEVEL = 4  newdate = 11/29/16 
 REPORTING LEVEL = 4  newdate = 11/29/16 
 REPORTING LEVEL = 4  newdate = 11/09/16 
 REPORTING LEVEL = 4  newdate = 11/09/16 
 REPORTING LEVEL = 4  newdate = 11/09/16 
 REPORTING LEVEL = 4  newdate = 11/09/16 
 REPORTING LEVEL = 4  newdate = 10/21/16 
 REPORTING LEVEL = 4  newdate = 10/21/16 
 REPORTING LEVEL = 4  newdate = 10/21/16 
 REPORTING LEVEL = 4  newdate = 10/21/16 
 REPORTING LEVEL = 4  newdate = 10/20/16 
 REPORTING LEVEL = 4  newdate = 10/20/16 
 REPORTING LEVEL = 4  newdate = 10/20/16 
 REPORTING LEVEL = 4  newdate = 10/20/16 
 REPORTING LEVEL = 4  newdate = 09/29/16 
 REPORTING LEVEL = 4  newdate = 09/29/16 
 REPORTING LEVEL = 4  newdate = 09/29/16 
 REPORTING LEVEL = 4  newdate = 09/29/16 
 REPORTING LEVEL = 4  newdate = 09/21/16 
 REPORTING LEVEL = 4  newdate = 09/21/16 
 REPORTING LEVEL = 4  newdate = 09/21/16 
 REPORTING LEVEL = 4  newdate = 09/21/16 
 REPORTING LEVEL = 4  newdate = 09/07/16 
 REPORTING LEVEL = 4  newdate = 09/07/16 
 REPORTING LEVEL = 4  newdate = 09/07/16 
 REPORTING LEVEL = 4  newdate = 09/07/16 
 REPORTING LEVEL = 4  newdate = 08/31/16 
 REPORTING LEVEL = 4  newdate = 08/31/16 
 REPORTING LEVEL = 4  newdate = 08/31/16 
 REPORTING LEVEL = 4  newdate = 08/31/16 
 REPORTING LEVEL = 4  newdate = 08/20/16 
 REPORTING LEVEL = 4  newdate = 08/20/16 
 REPORTING LEVEL = 4  newdate = 08/20/16 
 REPORTING LEVEL = 4  newdate = 08/20/16 
 REPORTING LEVEL = 4  newdate = 08/12/16 
 REPORTING LEVEL = 4  newdate = 08/12/16 
 REPORTING LEVEL = 4  newdate = 08/12/16 
 REPORTING LEVEL = 4  newdate = 08/12/16 
 REPORTING LEVEL = 4  newdate = 08/05/16 
 REPORTING LEVEL = 4  newdate = 08/05/16 
 REPORTING LEVEL = 4  newdate = 08/05/16 
 REPORTING LEVEL = 4  newdate = 08/05/16 
 REPORTING LEVEL = 4  newdate = 08/05/16 
 REPORTING LEVEL = 4  newdate = 08/05/16 
 REPORTING LEVEL = 4  newdate = 08/05/16 
 REPORTING LEVEL = 4  newdate = 08/05/16 
 REPORTING LEVEL = 4  newdate = 07/22/16 
 REPORTING LEVEL = 4  newdate = 07/22/16 
 REPORTING LEVEL = 4  newdate = 07/22/16 
 REPORTING LEVEL = 4  newdate = 07/22/16 
 REPORTING LEVEL = 4  newdate = 07/08/16 
 REPORTING LEVEL = 4  newdate = 07/08/16 
 REPORTING LEVEL = 4  newdate = 07/08/16 
 REPORTING LEVEL = 4  newdate = 07/08/16 
 REPORTING LEVEL = 4  newdate = 05/10/16 
 REPORTING LEVEL = 4  newdate = 05/10/16 
 REPORTING LEVEL = 4  newdate = 05/10/16 
 REPORTING LEVEL = 4  newdate = 05/10/16 
 REPORTING LEVEL = 4  newdate = 03/23/16 
 REPORTING LEVEL = 4  newdate = 03/23/16 
 REPORTING LEVEL = 4  newdate = 03/23/16 
 REPORTING LEVEL = 4  newdate = 03/23/16 
 REPORTING LEVEL = 4  newdate = 03/23/16 
 REPORTING LEVEL = 4  newdate = 03/23/16 
 REPORTING LEVEL = 4  newdate = 03/16/16 
 REPORTING LEVEL = 4  newdate = 03/16/16 
 REPORTING LEVEL = 4  newdate = 03/16/16 
 REPORTING LEVEL = 4  newdate = 03/16/16 
 REPORTING LEVEL = 4  newdate = 03/16/16 
 REPORTING LEVEL = 4  newdate = 03/16/16 
 REPORTING LEVEL = 4  newdate = 03/01/16 
 REPORTING LEVEL = 4  newdate = 03/01/16 
 REPORTING LEVEL = 4  newdate = 03/01/16 
 REPORTING LEVEL = 4  newdate = 03/01/16 
 REPORTING LEVEL = 4  newdate = 03/01/16 
 REPORTING LEVEL = 4  newdate = 03/01/16 
 REPORTING LEVEL = 4  newdate = 03/01/16 
 REPORTING LEVEL = 4  newdate = 03/01/16 
 REPORTING LEVEL = 4  newdate = 03/01/16 
 REPORTING LEVEL = 4  newdate = 03/01/16 
 REPORTING LEVEL = 4  newdate = 03/01/16 
 REPORTING LEVEL = 4  newdate = 03/01/16 
 REPORTING LEVEL = 4  newdate = 02/09/16 
 REPORTING LEVEL = 4  newdate = 02/09/16 
 REPORTING LEVEL = 4  newdate = 02/09/16 
 REPORTING LEVEL = 4  newdate = 02/09/16 
 REPORTING LEVEL = 4  newdate = 02/09/16 
 REPORTING LEVEL = 4  newdate = 02/09/16 
 REPORTING LEVEL = 4  newdate = 02/09/16 
 REPORTING LEVEL = 4  newdate = 02/09/16 
 REPORTING LEVEL = 4  newdate = 02/09/16 
 REPORTING LEVEL = 4  newdate = 02/09/16 
 REPORTING LEVEL = 4  newdate = 02/09/16 
 REPORTING LEVEL = 4  newdate = 02/09/16 
 REPORTING LEVEL = 4  newdate = 02/02/16 
 REPORTING LEVEL = 4  newdate = 02/02/16 
 REPORTING LEVEL = 4  newdate = 02/02/16 
 REPORTING LEVEL = 4  newdate = 02/02/16 
 REPORTING LEVEL = 4  newdate = 02/02/16 
 REPORTING LEVEL = 4  newdate = 02/02/16 
 REPORTING LEVEL = 4  newdate = 01/27/16 
 REPORTING LEVEL = 4  newdate = 01/27/16 
 REPORTING LEVEL = 4  newdate = 01/27/16 
 REPORTING LEVEL = 4  newdate = 01/27/16 
 REPORTING LEVEL = 4  newdate = 01/27/16 
 REPORTING LEVEL = 4
The SGPlot Procedure

Updated 08/13/2018

False Positive & Negative Listing for FIPRONIL

Status Lab ID Spike Mix Reporting Level Analysis Date Result Conc. Expected Conc.
False Negative 20161960006 Spex Organics TS160511023: 40 µl & ChemService 5154100: 40 µl & ChemService 5154 4 08/05/16 < 4 10
  20163420124 Abs 071816: 40 µl & Spex Organics TS160603008: 40 µl 4 12/13/16 < 4 10.04
  20171440225 Abs 071216: 40 µl & Abs 071816: 40 µl 4 05/27/17 < 5 10.04
  20172020151 Spex Organics TS160511023: 40 µl & Abs 071816: 40 µl 4 07/26/17 < 7.91 10.04
False Positive 20171300149 Spex Organics TS160511023: 40 µl & Spex Organics TS160603008: 40 µl 4 05/17/17 1.83 0
  20171720143 Spex Organics TS160511023: 40 µl & Spex Organics TS160603008: 40 µl 4 06/27/17 E 1.45 0

Updated 08/13/2018