Organic Blind Sample Program
False Positives & False Negatives
BUTYLATE
Method: 2437 Testid: 65068LCM60
Link to Individual Chart

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 newdate = 11/08/16 
 falseneg = -0.01  newdate = 10/06/16 
 falseneg = -0.01  newdate = 08/11/16 
 falseneg = -0.01  newdate = 08/11/16 
 falseneg = -0.01  newdate = 06/29/16 
 falseneg = -0.01  newdate = 06/29/16 
 falseneg = -0.01  newdate = 03/01/16 
 falseneg = -0.01  newdate = 10/11/17 
 CENC_VAL = 21.200  newdate = 10/04/17 
 CENC_VAL = 54.900  newdate = 09/23/17 
 CENC_VAL = 16.600  newdate = 08/23/17 
 CENC_VAL = 45.900  newdate = 08/08/17 
 CENC_VAL = 24.500  newdate = 07/28/17 
 CENC_VAL = 25.000  newdate = 07/19/17 
 CENC_VAL = 34.400  newdate = 07/12/17 
 CENC_VAL = 17.600  newdate = 07/11/17 
 CENC_VAL = 28.000  newdate = 07/08/17 
 CENC_VAL = 15.600  newdate = 06/24/17 
 CENC_VAL = 34.800  newdate = 06/07/17 
 CENC_VAL = 13.700  newdate = 06/05/17 
 CENC_VAL = 25.000  newdate = 06/02/17 
 CENC_VAL = 31.500  newdate = 05/17/17 
 CENC_VAL = 17.400  newdate = 03/10/17 
 CENC_VAL = 36.200  newdate = 03/10/17 
 CENC_VAL = 30.800  newdate = 02/16/17 
 CENC_VAL = 35.600  newdate = 02/16/17 
 CENC_VAL = 35.000  newdate = 02/01/17 
 CENC_VAL = 39.700  newdate = 02/01/17 
 CENC_VAL = 34.500  newdate = 01/18/17 
 CENC_VAL = 32.100  newdate = 01/17/17 
 CENC_VAL = 28.500  newdate = 01/04/17 
 CENC_VAL = 14.600  newdate = 01/04/17 
 CENC_VAL = 13.300  newdate = 12/13/16 
 CENC_VAL = 22.600  newdate = 12/13/16 
 CENC_VAL = 25.100  newdate = 11/22/16 
 CENC_VAL = 24.300  newdate = 11/22/16 
 CENC_VAL = 30.900  newdate = 11/11/16 
 CENC_VAL = 10.000  newdate = 11/11/16 
 CENC_VAL = 10.000  newdate = 11/09/16 
 CENC_VAL = 13.600  newdate = 11/08/16 
 CENC_VAL = 13.500  newdate = 11/08/16 
 CENC_VAL = 15.400  newdate = 10/06/16 
 CENC_VAL = 15.900  newdate = 09/21/16 
 CENC_VAL = 15.000  newdate = 09/21/16 
 CENC_VAL = 11.100  newdate = 09/13/16 
 CENC_VAL = 31.900  newdate = 09/13/16 
 CENC_VAL = 24.200  newdate = 08/31/16 
 CENC_VAL = 13.500  newdate = 08/30/16 
 CENC_VAL = 50.000  newdate = 08/24/16 
 CENC_VAL = 31.600  newdate = 08/24/16 
 CENC_VAL = 33.600  newdate = 08/03/16 
 CENC_VAL = 13.400  newdate = 08/03/16 
 CENC_VAL = 15.600  newdate = 07/29/16 
 CENC_VAL = 50.000  newdate = 07/29/16 
 CENC_VAL = 50.000  newdate = 07/12/16 
 CENC_VAL = 30.000  newdate = 07/12/16 
 CENC_VAL = 29.000  newdate = 05/06/16 
 CENC_VAL = 15.200  newdate = 05/06/16 
 CENC_VAL = 16.100  newdate = 03/23/16 
 CENC_VAL = 7.700  newdate = 03/23/16 
 CENC_VAL = 8.900  newdate = 03/23/16 
 CENC_VAL = 10.000  newdate = 03/17/16 
 CENC_VAL = 17.800  newdate = 03/17/16 
 CENC_VAL = 17.700  newdate = 03/17/16 
 CENC_VAL = 17.800  newdate = 03/02/16 
 CENC_VAL = 8.700  newdate = 03/02/16 
 CENC_VAL = 10.000  newdate = 03/02/16 
 CENC_VAL = 10.800  newdate = 03/01/16 
 CENC_VAL = 14.700  newdate = 03/01/16 
 CENC_VAL = 10.100  newdate = 02/19/16 
 CENC_VAL = 50.000  newdate = 02/19/16 
 CENC_VAL = 50.000  newdate = 02/19/16 
 CENC_VAL = 50.000  newdate = 02/18/16 
 CENC_VAL = 50.000  newdate = 02/18/16 
 CENC_VAL = 50.000  newdate = 02/18/16 
 CENC_VAL = 50.000  newdate = 02/17/16 
 CENC_VAL = 50.000  newdate = 02/17/16 
 CENC_VAL = 50.000  newdate = 02/17/16 
 CENC_VAL = 50.000  newdate = 02/12/16 
 CENC_VAL = 50.000  newdate = 02/12/16 
 CENC_VAL = 50.000  newdate = 02/12/16 
 CENC_VAL = 50.000  newdate = 10/11/17 
 REPORTING LEVEL = 10  newdate = 10/04/17 
 REPORTING LEVEL = 10  newdate = 10/04/17 
 REPORTING LEVEL = 10  newdate = 09/23/17 
 REPORTING LEVEL = 10  newdate = 09/23/17 
 REPORTING LEVEL = 10  newdate = 08/23/17 
 REPORTING LEVEL = 10  newdate = 08/23/17 
 REPORTING LEVEL = 10  newdate = 08/08/17 
 REPORTING LEVEL = 10  newdate = 08/08/17 
 REPORTING LEVEL = 10  newdate = 07/28/17 
 REPORTING LEVEL = 10  newdate = 07/28/17 
 REPORTING LEVEL = 10  newdate = 07/19/17 
 REPORTING LEVEL = 10  newdate = 07/19/17 
 REPORTING LEVEL = 10  newdate = 07/12/17 
 REPORTING LEVEL = 10  newdate = 07/12/17 
 REPORTING LEVEL = 10  newdate = 07/11/17 
 REPORTING LEVEL = 10  newdate = 07/11/17 
 REPORTING LEVEL = 10  newdate = 07/08/17 
 REPORTING LEVEL = 10  newdate = 07/08/17 
 REPORTING LEVEL = 10  newdate = 06/24/17 
 REPORTING LEVEL = 10  newdate = 06/24/17 
 REPORTING LEVEL = 10  newdate = 06/07/17 
 REPORTING LEVEL = 10  newdate = 06/07/17 
 REPORTING LEVEL = 10  newdate = 06/05/17 
 REPORTING LEVEL = 10  newdate = 06/05/17 
 REPORTING LEVEL = 10  newdate = 06/02/17 
 REPORTING LEVEL = 10  newdate = 06/02/17 
 REPORTING LEVEL = 10  newdate = 05/17/17 
 REPORTING LEVEL = 10  newdate = 05/17/17 
 REPORTING LEVEL = 10  newdate = 03/10/17 
 REPORTING LEVEL = 10  newdate = 03/10/17 
 REPORTING LEVEL = 10  newdate = 03/10/17 
 REPORTING LEVEL = 10  newdate = 03/10/17 
 REPORTING LEVEL = 10  newdate = 02/16/17 
 REPORTING LEVEL = 10  newdate = 02/16/17 
 REPORTING LEVEL = 10  newdate = 02/16/17 
 REPORTING LEVEL = 10  newdate = 02/16/17 
 REPORTING LEVEL = 10  newdate = 02/01/17 
 REPORTING LEVEL = 10  newdate = 02/01/17 
 REPORTING LEVEL = 10  newdate = 02/01/17 
 REPORTING LEVEL = 10  newdate = 02/01/17 
 REPORTING LEVEL = 10  newdate = 01/18/17 
 REPORTING LEVEL = 10  newdate = 01/18/17 
 REPORTING LEVEL = 10  newdate = 01/17/17 
 REPORTING LEVEL = 10  newdate = 01/17/17 
 REPORTING LEVEL = 10  newdate = 01/04/17 
 REPORTING LEVEL = 10  newdate = 01/04/17 
 REPORTING LEVEL = 10  newdate = 01/04/17 
 REPORTING LEVEL = 10  newdate = 01/04/17 
 REPORTING LEVEL = 10  newdate = 12/13/16 
 REPORTING LEVEL = 10  newdate = 12/13/16 
 REPORTING LEVEL = 10  newdate = 12/13/16 
 REPORTING LEVEL = 10  newdate = 12/13/16 
 REPORTING LEVEL = 10  newdate = 11/22/16 
 REPORTING LEVEL = 10  newdate = 11/22/16 
 REPORTING LEVEL = 10  newdate = 11/22/16 
 REPORTING LEVEL = 10  newdate = 11/22/16 
 REPORTING LEVEL = 10  newdate = 11/11/16 
 REPORTING LEVEL = 10  newdate = 11/11/16 
 REPORTING LEVEL = 10  newdate = 11/11/16 
 REPORTING LEVEL = 10  newdate = 11/11/16 
 REPORTING LEVEL = 10  newdate = 11/09/16 
 REPORTING LEVEL = 10  newdate = 11/09/16 
 REPORTING LEVEL = 10  newdate = 11/08/16 
 REPORTING LEVEL = 10  newdate = 11/08/16 
 REPORTING LEVEL = 10  newdate = 11/08/16 
 REPORTING LEVEL = 10  newdate = 11/08/16 
 REPORTING LEVEL = 10  newdate = 11/08/16 
 REPORTING LEVEL = 10  newdate = 11/08/16 
 REPORTING LEVEL = 10  newdate = 10/06/16 
 REPORTING LEVEL = 10  newdate = 10/06/16 
 REPORTING LEVEL = 10  newdate = 10/06/16 
 REPORTING LEVEL = 10  newdate = 10/06/16 
 REPORTING LEVEL = 10  newdate = 09/21/16 
 REPORTING LEVEL = 10  newdate = 09/21/16 
 REPORTING LEVEL = 10  newdate = 09/21/16 
 REPORTING LEVEL = 10  newdate = 09/21/16 
 REPORTING LEVEL = 10  newdate = 09/13/16 
 REPORTING LEVEL = 10  newdate = 09/13/16 
 REPORTING LEVEL = 10  newdate = 09/13/16 
 REPORTING LEVEL = 10  newdate = 09/13/16 
 REPORTING LEVEL = 10  newdate = 08/31/16 
 REPORTING LEVEL = 10  newdate = 08/31/16 
 REPORTING LEVEL = 10  newdate = 08/30/16 
 REPORTING LEVEL = 10  newdate = 08/30/16 
 REPORTING LEVEL = 10  newdate = 08/24/16 
 REPORTING LEVEL = 10  newdate = 08/24/16 
 REPORTING LEVEL = 10  newdate = 08/24/16 
 REPORTING LEVEL = 10  newdate = 08/24/16 
 REPORTING LEVEL = 10  newdate = 08/11/16 
 REPORTING LEVEL = 10  newdate = 08/11/16 
 REPORTING LEVEL = 10  newdate = 08/11/16 
 REPORTING LEVEL = 10  newdate = 08/11/16 
 REPORTING LEVEL = 10  newdate = 08/03/16 
 REPORTING LEVEL = 10  newdate = 08/03/16 
 REPORTING LEVEL = 10  newdate = 08/03/16 
 REPORTING LEVEL = 10  newdate = 08/03/16 
 REPORTING LEVEL = 10  newdate = 07/29/16 
 REPORTING LEVEL = 10  newdate = 07/29/16 
 REPORTING LEVEL = 10  newdate = 07/29/16 
 REPORTING LEVEL = 10  newdate = 07/29/16 
 REPORTING LEVEL = 10  newdate = 07/12/16 
 REPORTING LEVEL = 10  newdate = 07/12/16 
 REPORTING LEVEL = 10  newdate = 07/12/16 
 REPORTING LEVEL = 10  newdate = 07/12/16 
 REPORTING LEVEL = 10  newdate = 06/29/16 
 REPORTING LEVEL = 10  newdate = 06/29/16 
 REPORTING LEVEL = 10  newdate = 06/29/16 
 REPORTING LEVEL = 10  newdate = 06/29/16 
 REPORTING LEVEL = 10  newdate = 06/29/16 
 REPORTING LEVEL = 10  newdate = 06/29/16 
 REPORTING LEVEL = 10  newdate = 06/29/16 
 REPORTING LEVEL = 10  newdate = 06/29/16 
 REPORTING LEVEL = 10  newdate = 05/06/16 
 REPORTING LEVEL = 10  newdate = 05/06/16 
 REPORTING LEVEL = 10  newdate = 05/06/16 
 REPORTING LEVEL = 10  newdate = 05/06/16 
 REPORTING LEVEL = 10  newdate = 03/23/16 
 REPORTING LEVEL = 10  newdate = 03/23/16 
 REPORTING LEVEL = 10  newdate = 03/23/16 
 REPORTING LEVEL = 10  newdate = 03/23/16 
 REPORTING LEVEL = 10  newdate = 03/23/16 
 REPORTING LEVEL = 10  newdate = 03/23/16 
 REPORTING LEVEL = 10  newdate = 03/17/16 
 REPORTING LEVEL = 10  newdate = 03/17/16 
 REPORTING LEVEL = 10  newdate = 03/17/16 
 REPORTING LEVEL = 10  newdate = 03/17/16 
 REPORTING LEVEL = 10  newdate = 03/17/16 
 REPORTING LEVEL = 10  newdate = 03/17/16 
 REPORTING LEVEL = 10  newdate = 03/02/16 
 REPORTING LEVEL = 10  newdate = 03/02/16 
 REPORTING LEVEL = 10  newdate = 03/02/16 
 REPORTING LEVEL = 10  newdate = 03/02/16 
 REPORTING LEVEL = 10  newdate = 03/02/16 
 REPORTING LEVEL = 10  newdate = 03/02/16 
 REPORTING LEVEL = 10  newdate = 03/01/16 
 REPORTING LEVEL = 10  newdate = 03/01/16 
 REPORTING LEVEL = 10  newdate = 03/01/16 
 REPORTING LEVEL = 10  newdate = 03/01/16 
 REPORTING LEVEL = 10  newdate = 03/01/16 
 REPORTING LEVEL = 10  newdate = 03/01/16 
 REPORTING LEVEL = 10  newdate = 02/19/16 
 REPORTING LEVEL = 10  newdate = 02/19/16 
 REPORTING LEVEL = 10  newdate = 02/19/16 
 REPORTING LEVEL = 10  newdate = 02/19/16 
 REPORTING LEVEL = 10  newdate = 02/19/16 
 REPORTING LEVEL = 10  newdate = 02/19/16 
 REPORTING LEVEL = 10  newdate = 02/18/16 
 REPORTING LEVEL = 10  newdate = 02/18/16 
 REPORTING LEVEL = 10  newdate = 02/18/16 
 REPORTING LEVEL = 10  newdate = 02/18/16 
 REPORTING LEVEL = 10  newdate = 02/18/16 
 REPORTING LEVEL = 10  newdate = 02/18/16 
 REPORTING LEVEL = 10  newdate = 02/17/16 
 REPORTING LEVEL = 10  newdate = 02/17/16 
 REPORTING LEVEL = 10  newdate = 02/17/16 
 REPORTING LEVEL = 10  newdate = 02/17/16 
 REPORTING LEVEL = 10  newdate = 02/17/16 
 REPORTING LEVEL = 10  newdate = 02/17/16 
 REPORTING LEVEL = 10  newdate = 02/12/16 
 REPORTING LEVEL = 10  newdate = 02/12/16 
 REPORTING LEVEL = 10  newdate = 02/12/16 
 REPORTING LEVEL = 10  newdate = 02/12/16 
 REPORTING LEVEL = 10  newdate = 02/12/16 
 REPORTING LEVEL = 10
The SGPlot Procedure

Updated 08/13/2018

False Positive & Negative Listing for BUTYLATE

Status Lab ID Spike Mix Reporting Level Analysis Date Result Conc. Expected Conc.
False Negative 20160490029 ChemService 3995200: 20 µl & ChemService 3880100: 20 µl & ChemService 4047100: 2 10 03/01/16 < 12.3 18.2
  20161740280 Spex Organics TS160511023: 40 µl & ChemService 5154100: 40 µl & ChemService 5154 10 06/29/16 < 10 14.88
  20161740281 Spex Organics TS160511023: 40 µl & ChemService 5154100: 40 µl & ChemService 5154 10 06/29/16 < 10 14.88
  20162150206 Spex Organics TS160511023: 40 µl & ChemService 5154100: 40 µl & ChemService 5154 10 08/11/16 < 10 14.88
  20162150207 Spex Organics TS160511023: 40 µl & ChemService 5154100: 40 µl & ChemService 5154 10 08/11/16 < 10 14.88
  20162720260 Spex Organics TS160603008: 40 µl & Abs 071216: 40 µl 10 10/06/16 < 14.3 14.84
  20162990150 Abs 072516: 40 µl & Abs 071216: 40 µl 10 11/08/16 < 14.5 14.84

Updated 08/13/2018