OBSP Spike Level Charts

OBSP Determination:

11-KETOTESTOSTERONE

METHOD: 4434 , TESTIDCODE: 64527GM005

Plotted Points Statistics

11-KETOTESTOSTERONE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	38	90%	19%	88%	15%
Total	38	90%	19%	88%	15%

Sample Statistics

11-KETOTESTOSTERONE

Characteristic	N	%	% Basis
Plotted	38	81%	Spiked
Estimated Values	1	2%	Spiked
Deleted Values	0	0%	Spiked + Not Spiked
Spiked, Censored	5	11%	Spiked
Spiked	47	.
False Negatives	4	9%	4 out of 47
Not Spiked	69	.
False Positives	0	0%	0 out of 69

OBSP Determination:

17-ALPHA-ESTRADIOL

METHOD: 4434 , TESTIDCODE: 64528GM005

Plotted Points Statistics

17-ALPHA-ESTRADIOL

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	68	87%	26%	84%	13%
Total	68	87%	26%	84%	13%

Sample Statistics

17-ALPHA-ESTRADIOL

Characteristic	N	%	% Basis
Plotted	68	89%	Spiked
Estimated Values	0	0%	Spiked
Deleted Values	0	0%	Spiked + Not Spiked
Spiked, Censored	3	4%	Spiked
Spiked	76	.
False Negatives	5	7%	5 out of 76
Not Spiked	40	.
False Positives	1	3%	1 out of 40

OBSP Determination:

17-ALPHA-ETHYNYLESTRADIOL

METHOD: 4434 , TESTIDCODE: 64529GM005

Plotted Points Statistics

17-ALPHA-ETHYNYLESTRADIOL

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	58	80%	17%	78%	15%
Total	58	80%	17%	78%	15%

Sample Statistics

17-ALPHA-ETHYNYLESTRADIOL

Characteristic	N	%	% Basis
Plotted	58	76%	Spiked
Estimated Values	1	1%	Spiked
Deleted Values	0	0%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	76	.
False Negatives	18	24%	18 out of 76
Not Spiked	40	.
False Positives	2	5%	2 out of 40

OBSP Determination:

17-BETA-ESTRADIOL

METHOD: 4434 , TESTIDCODE: 64530GM005

Plotted Points Statistics

17-BETA-ESTRADIOL

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	54	78%	12%	79%	9%
Total	54	78%	12%	79%	9%

Sample Statistics

17-BETA-ESTRADIOL

Characteristic	N	%	% Basis
Plotted	54	78%	Spiked
Estimated Values	0	0%	Spiked
Deleted Values	0	0%	Spiked + Not Spiked
Spiked, Censored	1	1%	Spiked
Spiked	69	.
False Negatives	14	20%	14 out of 69
Not Spiked	39	.
False Positives	1	3%	1 out of 39

OBSP Determination:

3-BETA-COPROSTANOL

METHOD: 4434 , TESTIDCODE: 64532GM005

Plotted Points Statistics

3-BETA-COPROSTANOL

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	30	70%	20%	62%	21%
Total	30	70%	20%	62%	21%

Sample Statistics

3-BETA-COPROSTANOL

Characteristic	N	%	% Basis
Plotted	30	65%	Spiked
Estimated Values	2	4%	Spiked
Deleted Values	1	1%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	47	.
False Negatives	16	35%	16 out of 46
Not Spiked	25	.
False Positives	0	0%	0 out of 25

OBSP Determination:

4,4^-BISPHENOL F

METHOD: 4434 , TESTIDCODE: 51294GM005

Plotted Points Statistics

4,4^-BISPHENOL F

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	32	85%	30%	80%	28%
Total	32	85%	30%	80%	28%

Sample Statistics

4,4^-BISPHENOL F

Characteristic	N	%	% Basis
Plotted	32	100%	Spiked
Estimated Values	32	100%	Spiked
Deleted Values	0	0%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	32	.
False Negatives	0	0%	0 out of 32
Not Spiked	61	.
False Positives	0	0%	0 out of 61

OBSP Determination:

4,4^-BISPHENOL F, WU

METHOD: 4434 , TESTIDCODE: 51294GM005

Plotted Points Statistics

4,4^-BISPHENOL F, WU

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	32	85%	30%	80%	28%
Total	32	85%	30%	80%	28%

Sample Statistics

4,4^-BISPHENOL F, WU

Characteristic	N	%	% Basis
Plotted	32	100%	Spiked
Estimated Values	32	100%	Spiked
Deleted Values	0	0%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	32	.
False Negatives	0	0%	0 out of 32
Not Spiked	61	.
False Positives	0	0%	0 out of 61

OBSP Determination:

4,4^-BISPHENOL S

METHOD: 4434 , TESTIDCODE: 51295GM005

Sample Statistics

4,4^-BISPHENOL S

Characteristic	N	%	% Basis
Plotted	0	.	Spiked
Estimated Values	0	.	Spiked
Deleted Values	4	100%	Spiked + Not Spiked
Spiked, Censored	0	.	Spiked
Spiked	0	.
False Negatives	0	.	0 out of 0
Not Spiked	4	.
False Positives	0	.	0 out of 0

OBSP Determination:

4-ANDROSTENE-3,17-DIONE

METHOD: 4434 , TESTIDCODE: 64533GM005

Plotted Points Statistics

4-ANDROSTENE-3,17-DIONE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	28	61%	27%	56%	20%
Total	28	61%	27%	56%	20%

Sample Statistics

4-ANDROSTENE-3,17-DIONE

Characteristic	N	%	% Basis
Plotted	28	64%	Spiked
Estimated Values	1	2%	Spiked
Deleted Values	0	0%	Spiked + Not Spiked
Spiked, Censored	8	18%	Spiked
Spiked	44	.
False Negatives	8	18%	8 out of 44
Not Spiked	72	.
False Positives	1	1%	1 out of 72

OBSP Determination:

BISPHENOL A

METHOD: 4434 , TESTIDCODE: 67305GM005

Plotted Points Statistics

BISPHENOL A

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	40	79%	24%	80%	26%
Total	40	79%	24%	80%	26%

Sample Statistics

BISPHENOL A

Characteristic	N	%	% Basis
Plotted	40	95%	Spiked
Estimated Values	27	64%	Spiked
Deleted Values	2	3%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	43	.
False Negatives	2	5%	2 out of 42
Not Spiked	29	.
False Positives	0	0%	0 out of 28

OBSP Determination:

CHOLESTEROL

METHOD: 4434 , TESTIDCODE: 64534GM005

Plotted Points Statistics

CHOLESTEROL

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	42	81%	20%	75%	15%
Total	42	81%	20%	75%	15%

Sample Statistics

CHOLESTEROL

Characteristic	N	%	% Basis
Plotted	42	93%	Spiked
Estimated Values	0	0%	Spiked
Deleted Values	1	1%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	46	.
False Negatives	3	7%	3 out of 45
Not Spiked	26	.
False Positives	2	8%	2 out of 26

OBSP Determination:

CIS-ANDROSTERONE

METHOD: 4434 , TESTIDCODE: 64535GM005

Plotted Points Statistics

CIS-ANDROSTERONE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
< Reporting Level	3	63%	8%	61%	11%
>= Reporting Level	57	69%	18%	66%	21%
Total	60	69%	18%	66%	20%

Sample Statistics

CIS-ANDROSTERONE

Characteristic	N	%	% Basis
Plotted	60	81%	Spiked
Estimated Values	0	0%	Spiked
Deleted Values	0	0%	Spiked + Not Spiked
Spiked, Censored	5	7%	Spiked
Spiked	74	.
False Negatives	9	12%	9 out of 74
Not Spiked	42	.
False Positives	1	2%	1 out of 42

OBSP Determination:

DIHYDROTESTOSTERONE

METHOD: 4434 , TESTIDCODE: 64544GM005

Plotted Points Statistics

DIHYDROTESTOSTERONE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	49	71%	18%	73%	13%
Total	49	71%	18%	73%	13%

Sample Statistics

DIHYDROTESTOSTERONE

Characteristic	N	%	% Basis
Plotted	49	79%	Spiked
Estimated Values	2	3%	Spiked
Deleted Values	0	0%	Spiked + Not Spiked
Spiked, Censored	3	5%	Spiked
Spiked	62	.
False Negatives	10	16%	10 out of 62
Not Spiked	54	.
False Positives	1	2%	1 out of 54

OBSP Determination:

EPITESTOSTERONE

METHOD: 4434 , TESTIDCODE: 64537GM005

Plotted Points Statistics

EPITESTOSTERONE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	60	70%	18%	68%	11%
Total	60	70%	18%	68%	11%

Sample Statistics

EPITESTOSTERONE

Characteristic	N	%	% Basis
Plotted	60	90%	Spiked
Estimated Values	4	6%	Spiked
Deleted Values	0	0%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	67	.
False Negatives	7	10%	7 out of 67
Not Spiked	49	.
False Positives	0	0%	0 out of 49

OBSP Determination:

EQUILENIN

METHOD: 4434 , TESTIDCODE: 64538GM005

Plotted Points Statistics

EQUILENIN

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	44	95%	37%	102%	43%
Total	44	95%	37%	102%	43%

Sample Statistics

EQUILENIN

Characteristic	N	%	% Basis
Plotted	44	100%	Spiked
Estimated Values	3	7%	Spiked
Deleted Values	0	0%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	44	.
False Negatives	0	0%	0 out of 44
Not Spiked	27	.
False Positives	0	0%	0 out of 27

OBSP Determination:

EQUILIN

METHOD: 4434 , TESTIDCODE: 64539GM005

Plotted Points Statistics

EQUILIN

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	63	63%	20%	61%	16%
Total	63	63%	20%	61%	16%

Sample Statistics

EQUILIN

Characteristic	N	%	% Basis
Plotted	63	85%	Spiked
Estimated Values	63	85%	Spiked
Deleted Values	0	0%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	74	.
False Negatives	11	15%	11 out of 74
Not Spiked	42	.
False Positives	0	0%	0 out of 42

OBSP Determination:

ESTRIOL

METHOD: 4434 , TESTIDCODE: 64540GM005

Plotted Points Statistics

ESTRIOL

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	69	80%	16%	81%	16%
Total	69	80%	16%	81%	16%

Sample Statistics

ESTRIOL

Characteristic	N	%	% Basis
Plotted	69	91%	Spiked
Estimated Values	0	0%	Spiked
Deleted Values	0	0%	Spiked + Not Spiked
Spiked, Censored	1	1%	Spiked
Spiked	76	.
False Negatives	6	8%	6 out of 76
Not Spiked	40	.
False Positives	0	0%	0 out of 40

OBSP Determination:

ESTRONE

METHOD: 4434 , TESTIDCODE: 64541GM005

Plotted Points Statistics

ESTRONE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	59	71%	17%	68%	15%
Total	59	71%	17%	68%	15%

Sample Statistics

ESTRONE

Characteristic	N	%	% Basis
Plotted	59	73%	Spiked
Estimated Values	5	6%	Spiked
Deleted Values	1	1%	Spiked + Not Spiked
Spiked, Censored	6	7%	Spiked
Spiked	81	.
False Negatives	16	20%	16 out of 81
Not Spiked	35	.
False Positives	0	0%	0 out of 34

OBSP Determination:

MESTRANOL

METHOD: 4434 , TESTIDCODE: 64542GM005

Plotted Points Statistics

MESTRANOL

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	35	48%	22%	44%	14%
Total	35	48%	22%	44%	14%

Sample Statistics

MESTRANOL

Characteristic	N	%	% Basis
Plotted	35	47%	Spiked
Estimated Values	2	3%	Spiked
Deleted Values	0	0%	Spiked + Not Spiked
Spiked, Censored	3	4%	Spiked
Spiked	75	.
False Negatives	37	49%	37 out of 75
Not Spiked	38	.
False Positives	2	5%	2 out of 38

OBSP Determination:

NORETHINDRONE

METHOD: 4434 , TESTIDCODE: 64531GM005

Plotted Points Statistics

NORETHINDRONE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	53	80%	19%	78%	15%
Total	53	80%	19%	78%	15%

Sample Statistics

NORETHINDRONE

Characteristic	N	%	% Basis
Plotted	53	70%	Spiked
Estimated Values	1	1%	Spiked
Deleted Values	0	0%	Spiked + Not Spiked
Spiked, Censored	3	4%	Spiked
Spiked	76	.
False Negatives	20	26%	20 out of 76
Not Spiked	40	.
False Positives	0	0%	0 out of 40

OBSP Determination:

PROGESTERONE

METHOD: 4434 , TESTIDCODE: 64543GM005

Plotted Points Statistics

PROGESTERONE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	64	40%	12%	38%	11%
Total	64	40%	12%	38%	11%

Sample Statistics

PROGESTERONE

Characteristic	N	%	% Basis
Plotted	64	82%	Spiked
Estimated Values	64	82%	Spiked
Deleted Values	0	0%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	78	.
False Negatives	14	18%	14 out of 78
Not Spiked	38	.
False Positives	0	0%	0 out of 38

OBSP Determination:

TESTOSTERONE

METHOD: 4434 , TESTIDCODE: 64545GM005

Plotted Points Statistics

TESTOSTERONE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	57	73%	13%	73%	13%
Total	57	73%	13%	73%	13%

Sample Statistics

TESTOSTERONE

Characteristic	N	%	% Basis
Plotted	57	84%	Spiked
Estimated Values	1	1%	Spiked
Deleted Values	0	0%	Spiked + Not Spiked
Spiked, Censored	1	1%	Spiked
Spiked	68	.
False Negatives	10	15%	10 out of 68
Not Spiked	45	.
False Positives	2	4%	2 out of 45

OBSP Determination:

TRANS-DIETHYLSTILBESTROL

METHOD: 4434 , TESTIDCODE: 64536GM005

Plotted Points Statistics

TRANS-DIETHYLSTILBESTROL

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	42	68%	14%	69%	15%
Total	42	68%	14%	69%	15%

Sample Statistics

TRANS-DIETHYLSTILBESTROL

Characteristic	N	%	% Basis
Plotted	42	86%	Spiked
Estimated Values	0	0%	Spiked
Deleted Values	0	0%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	49	.
False Negatives	7	14%	7 out of 49
Not Spiked	23	.
False Positives	0	0%	0 out of 23