OBSP Determination:
ISOQUINOLINE
METHOD: 4433 , TESTIDCODE: 62826GCM99

Laboratory ID = 20131020082 Lab Value = 0.458 Expected Conc. = 0.5 Report level label = 0.04 Pct Recovery = 92% Analysis Date = 05/30/13 SpikeMix = ChemService 426100: 40 µl & Spex Organics T1120521007: 40 µl SpecificMix = T1120521007 Laboratory ID = 20130250062 Lab Value = 0.368 Expected Conc. = 0.5 Report level label = 0.04 Pct Recovery = 74% Analysis Date = 02/07/13 SpikeMix = Spex Organics T1120521007: 40 µl & Supelco LB92782: 40 µl SpecificMix = T1120521007 Laboratory ID = 20130870086 Lab Value = 0.184 Expected Conc. = 0.25 Report level label = 0.04 Pct Recovery = 74% Analysis Date = 05/29/13 SpikeMix = NSI 061412-01: 20 µl & Crescent 05BB045: 20 µl SpecificMix = 061412-01 Laboratory ID = 20130460007 Lab Value = 0.172 Expected Conc. = 0.25 Report level label = 0.04 Pct Recovery = 69% Analysis Date = 03/27/13 SpikeMix = Spex Organics T1120521007: 20 µl & ChemService 426100: 20 µl SpecificMix = T1120521007 Laboratory ID = 20131440104 Lab Value = 0.100 Expected Conc. = 0.155 Report level label = 0.04 Pct Recovery = 65% Analysis Date = 06/14/13 SpikeMix = NSI 042213WWUF: 50 µl & Supelco LC00152: 50 µl SpecificMix = 042213WWUF Laboratory ID = 20131290118 Lab Value = 0.124 Expected Conc. = 0.155 Report level label = 0.04 Pct Recovery = 80% Analysis Date = 06/12/13 SpikeMix = NSI 042213WWUF: 50 µl & ChemService 1466200: 50 µl SpecificMix = 042213WWUF Laboratory ID = 20132910006 Lab Value = 0.062 Expected Conc. = 0.062 Report level label = 0.04 Pct Recovery = 100% Analysis Date = 11/14/13 SpikeMix = NSI 042213WWUF: 20 µl & Crescent 04CC095: 20 µl SpecificMix = 042213WWUF Laboratory ID = 20132560002 Lab Value = 0.067 Expected Conc. = 0.062 Report level label = 0.04 Pct Recovery = 108% Analysis Date = 09/26/13 SpikeMix = NSI 042213WWUF: 20 µl & Abs 050613WWUF: 20 µl SpecificMix = 042213WWUF Analysis Date = 11/14/13 Pct Recovery = 100% Analysis Date = 11/12/13 Pct Recovery = 100% Analysis Date = 11/12/13 Pct Recovery = 100% Analysis Date = 11/11/13 Pct Recovery = 100% Analysis Date = 11/11/13 Pct Recovery = 100% Analysis Date = 11/09/13 Pct Recovery = 101% Analysis Date = 11/09/13 Pct Recovery = 101% Analysis Date = 11/08/13 Pct Recovery = 101% Analysis Date = 11/08/13 Pct Recovery = 101% Analysis Date = 11/07/13 Pct Recovery = 101% Analysis Date = 11/07/13 Pct Recovery = 101% Analysis Date = 11/05/13 Pct Recovery = 101% Analysis Date = 11/05/13 Pct Recovery = 101% Analysis Date = 11/04/13 Pct Recovery = 102% Analysis Date = 11/04/13 Pct Recovery = 102% Analysis Date = 11/02/13 Pct Recovery = 102% Analysis Date = 11/02/13 Pct Recovery = 102% Analysis Date = 11/01/13 Pct Recovery = 102% Analysis Date = 11/01/13 Pct Recovery = 102% Analysis Date = 10/31/13 Pct Recovery = 102% Analysis Date = 10/31/13 Pct Recovery = 102% Analysis Date = 10/29/13 Pct Recovery = 103% Analysis Date = 10/29/13 Pct Recovery = 103% Analysis Date = 10/28/13 Pct Recovery = 103% Analysis Date = 10/28/13 Pct Recovery = 103% Analysis Date = 10/26/13 Pct Recovery = 103% Analysis Date = 10/26/13 Pct Recovery = 103% Analysis Date = 10/25/13 Pct Recovery = 103% Analysis Date = 10/25/13 Pct Recovery = 103% Analysis Date = 10/24/13 Pct Recovery = 103% Analysis Date = 10/24/13 Pct Recovery = 103% Analysis Date = 10/22/13 Pct Recovery = 104% Analysis Date = 10/22/13 Pct Recovery = 104% Analysis Date = 10/21/13 Pct Recovery = 104% Analysis Date = 10/21/13 Pct Recovery = 104% Analysis Date = 10/19/13 Pct Recovery = 104% Analysis Date = 10/19/13 Pct Recovery = 104% Analysis Date = 10/18/13 Pct Recovery = 104% Analysis Date = 10/18/13 Pct Recovery = 104% Analysis Date = 10/17/13 Pct Recovery = 105% Analysis Date = 10/17/13 Pct Recovery = 105% Analysis Date = 10/15/13 Pct Recovery = 105% Analysis Date = 10/15/13 Pct Recovery = 105% Analysis Date = 10/14/13 Pct Recovery = 105% Analysis Date = 10/14/13 Pct Recovery = 105% Analysis Date = 10/12/13 Pct Recovery = 105% Analysis Date = 10/12/13 Pct Recovery = 105% Analysis Date = 10/11/13 Pct Recovery = 106% Analysis Date = 10/11/13 Pct Recovery = 106% Analysis Date = 10/10/13 Pct Recovery = 106% Analysis Date = 10/10/13 Pct Recovery = 106% Analysis Date = 10/08/13 Pct Recovery = 106% Analysis Date = 10/08/13 Pct Recovery = 106% Analysis Date = 10/07/13 Pct Recovery = 106% Analysis Date = 10/07/13 Pct Recovery = 106% Analysis Date = 10/05/13 Pct Recovery = 106% Analysis Date = 10/05/13 Pct Recovery = 106% Analysis Date = 10/04/13 Pct Recovery = 107% Analysis Date = 10/04/13 Pct Recovery = 107% Analysis Date = 10/03/13 Pct Recovery = 107% Analysis Date = 10/03/13 Pct Recovery = 107% Analysis Date = 10/01/13 Pct Recovery = 107% Analysis Date = 10/01/13 Pct Recovery = 107% Analysis Date = 09/30/13 Pct Recovery = 107% Analysis Date = 09/30/13 Pct Recovery = 107% Analysis Date = 09/28/13 Pct Recovery = 108% Analysis Date = 09/28/13 Pct Recovery = 108% Analysis Date = 09/27/13 Pct Recovery = 108% Analysis Date = 09/27/13 Pct Recovery = 108% Analysis Date = 09/26/13 Pct Recovery = 108% Analysis Date = 09/26/13 Pct Recovery = 108% Analysis Date = 09/24/13 Pct Recovery = 107% Analysis Date = 09/24/13 Pct Recovery = 107% Analysis Date = 09/23/13 Pct Recovery = 107% Analysis Date = 09/23/13 Pct Recovery = 107% Analysis Date = 09/21/13 Pct Recovery = 106% Analysis Date = 09/21/13 Pct Recovery = 106% Analysis Date = 09/20/13 Pct Recovery = 106% Analysis Date = 09/20/13 Pct Recovery = 106% Analysis Date = 09/19/13 Pct Recovery = 105% Analysis Date = 09/19/13 Pct Recovery = 105% Analysis Date = 09/17/13 Pct Recovery = 105% Analysis Date = 09/17/13 Pct Recovery = 105% Analysis Date = 09/16/13 Pct Recovery = 104% Analysis Date = 09/16/13 Pct Recovery = 104% Analysis Date = 09/14/13 Pct Recovery = 104% Analysis Date = 09/14/13 Pct Recovery = 104% Analysis Date = 09/13/13 Pct Recovery = 103% Analysis Date = 09/13/13 Pct Recovery = 103% Analysis Date = 09/12/13 Pct Recovery = 102% Analysis Date = 09/12/13 Pct Recovery = 102% Analysis Date = 09/10/13 Pct Recovery = 102% Analysis Date = 09/10/13 Pct Recovery = 102% Analysis Date = 09/09/13 Pct Recovery = 101% Analysis Date = 09/09/13 Pct Recovery = 101% Analysis Date = 09/07/13 Pct Recovery = 101% Analysis Date = 09/07/13 Pct Recovery = 101% Analysis Date = 09/06/13 Pct Recovery = 100% Analysis Date = 09/06/13 Pct Recovery = 100% Analysis Date = 09/05/13 Pct Recovery = 100% Analysis Date = 09/05/13 Pct Recovery = 100% Analysis Date = 09/03/13 Pct Recovery = 99% Analysis Date = 09/03/13 Pct Recovery = 99% Analysis Date = 09/02/13 Pct Recovery = 99% Analysis Date = 09/02/13 Pct Recovery = 99% Analysis Date = 08/31/13 Pct Recovery = 98% Analysis Date = 08/31/13 Pct Recovery = 98% Analysis Date = 08/30/13 Pct Recovery = 97% Analysis Date = 08/30/13 Pct Recovery = 97% Analysis Date = 08/29/13 Pct Recovery = 97% Analysis Date = 08/29/13 Pct Recovery = 97% Analysis Date = 08/27/13 Pct Recovery = 96% Analysis Date = 08/27/13 Pct Recovery = 96% Analysis Date = 08/26/13 Pct Recovery = 96% Analysis Date = 08/26/13 Pct Recovery = 96% Analysis Date = 08/24/13 Pct Recovery = 95% Analysis Date = 08/24/13 Pct Recovery = 95% Analysis Date = 08/23/13 Pct Recovery = 95% Analysis Date = 08/23/13 Pct Recovery = 95% Analysis Date = 08/22/13 Pct Recovery = 94% Analysis Date = 08/22/13 Pct Recovery = 94% Analysis Date = 08/20/13 Pct Recovery = 94% Analysis Date = 08/20/13 Pct Recovery = 94% Analysis Date = 08/19/13 Pct Recovery = 93% Analysis Date = 08/19/13 Pct Recovery = 93% Analysis Date = 08/17/13 Pct Recovery = 92% Analysis Date = 08/17/13 Pct Recovery = 92% Analysis Date = 08/16/13 Pct Recovery = 92% Analysis Date = 08/16/13 Pct Recovery = 92% Analysis Date = 08/15/13 Pct Recovery = 91% Analysis Date = 08/15/13 Pct Recovery = 91% Analysis Date = 08/13/13 Pct Recovery = 91% Analysis Date = 08/13/13 Pct Recovery = 91% Analysis Date = 08/12/13 Pct Recovery = 90% Analysis Date = 08/12/13 Pct Recovery = 90% Analysis Date = 08/10/13 Pct Recovery = 90% Analysis Date = 08/10/13 Pct Recovery = 90% Analysis Date = 08/09/13 Pct Recovery = 89% Analysis Date = 08/09/13 Pct Recovery = 89% Analysis Date = 08/08/13 Pct Recovery = 88% Analysis Date = 08/08/13 Pct Recovery = 88% Analysis Date = 08/06/13 Pct Recovery = 88% Analysis Date = 08/06/13 Pct Recovery = 88% Analysis Date = 08/05/13 Pct Recovery = 87% Analysis Date = 08/05/13 Pct Recovery = 87% Analysis Date = 08/03/13 Pct Recovery = 87% Analysis Date = 08/03/13 Pct Recovery = 87% Analysis Date = 08/02/13 Pct Recovery = 86% Analysis Date = 08/02/13 Pct Recovery = 86% Analysis Date = 08/01/13 Pct Recovery = 86% Analysis Date = 08/01/13 Pct Recovery = 86% Analysis Date = 07/30/13 Pct Recovery = 85% Analysis Date = 07/30/13 Pct Recovery = 85% Analysis Date = 07/29/13 Pct Recovery = 85% Analysis Date = 07/29/13 Pct Recovery = 85% Analysis Date = 07/27/13 Pct Recovery = 84% Analysis Date = 07/27/13 Pct Recovery = 84% Analysis Date = 07/26/13 Pct Recovery = 83% Analysis Date = 07/26/13 Pct Recovery = 83% Analysis Date = 07/25/13 Pct Recovery = 83% Analysis Date = 07/25/13 Pct Recovery = 83% Analysis Date = 07/23/13 Pct Recovery = 82% Analysis Date = 07/23/13 Pct Recovery = 82% Analysis Date = 07/22/13 Pct Recovery = 82% Analysis Date = 07/22/13 Pct Recovery = 82% Analysis Date = 07/20/13 Pct Recovery = 81% Analysis Date = 07/20/13 Pct Recovery = 81% Analysis Date = 07/19/13 Pct Recovery = 81% Analysis Date = 07/19/13 Pct Recovery = 81% Analysis Date = 07/18/13 Pct Recovery = 80% Analysis Date = 07/18/13 Pct Recovery = 80% Analysis Date = 07/16/13 Pct Recovery = 80% Analysis Date = 07/16/13 Pct Recovery = 80% Analysis Date = 07/15/13 Pct Recovery = 79% Analysis Date = 07/15/13 Pct Recovery = 79% Analysis Date = 07/13/13 Pct Recovery = 78% Analysis Date = 07/13/13 Pct Recovery = 78% Analysis Date = 07/12/13 Pct Recovery = 78% Analysis Date = 07/12/13 Pct Recovery = 78% Analysis Date = 07/11/13 Pct Recovery = 77% Analysis Date = 07/11/13 Pct Recovery = 77% Analysis Date = 07/09/13 Pct Recovery = 77% Analysis Date = 07/09/13 Pct Recovery = 77% Analysis Date = 07/08/13 Pct Recovery = 76% Analysis Date = 07/08/13 Pct Recovery = 76% Analysis Date = 07/06/13 Pct Recovery = 76% Analysis Date = 07/06/13 Pct Recovery = 76% Analysis Date = 07/05/13 Pct Recovery = 75% Analysis Date = 07/05/13 Pct Recovery = 75% Analysis Date = 07/04/13 Pct Recovery = 75% Analysis Date = 07/04/13 Pct Recovery = 75% Analysis Date = 07/02/13 Pct Recovery = 74% Analysis Date = 07/02/13 Pct Recovery = 74% Analysis Date = 07/01/13 Pct Recovery = 73% Analysis Date = 07/01/13 Pct Recovery = 73% Analysis Date = 06/29/13 Pct Recovery = 73% Analysis Date = 06/29/13 Pct Recovery = 73% Analysis Date = 06/28/13 Pct Recovery = 72% Analysis Date = 06/28/13 Pct Recovery = 72% Analysis Date = 06/27/13 Pct Recovery = 72% Analysis Date = 06/27/13 Pct Recovery = 72% Analysis Date = 06/25/13 Pct Recovery = 71% Analysis Date = 06/25/13 Pct Recovery = 71% Analysis Date = 06/24/13 Pct Recovery = 71% Analysis Date = 06/24/13 Pct Recovery = 71% Analysis Date = 06/22/13 Pct Recovery = 70% Analysis Date = 06/22/13 Pct Recovery = 70% Analysis Date = 06/21/13 Pct Recovery = 70% Analysis Date = 06/21/13 Pct Recovery = 70% Analysis Date = 06/20/13 Pct Recovery = 69% Analysis Date = 06/20/13 Pct Recovery = 69% Analysis Date = 06/18/13 Pct Recovery = 68% Analysis Date = 06/18/13 Pct Recovery = 68% Analysis Date = 06/17/13 Pct Recovery = 68% Analysis Date = 06/17/13 Pct Recovery = 68% Analysis Date = 06/15/13 Pct Recovery = 67% Analysis Date = 06/15/13 Pct Recovery = 67% Analysis Date = 06/14/13 Pct Recovery = 67% Analysis Date = 06/14/13 Pct Recovery = 67% Analysis Date = 06/13/13 Pct Recovery = 72% Analysis Date = 06/13/13 Pct Recovery = 72% Analysis Date = 06/11/13 Pct Recovery = 77% Analysis Date = 06/11/13 Pct Recovery = 77% Analysis Date = 06/10/13 Pct Recovery = 78% Analysis Date = 06/10/13 Pct Recovery = 78% Analysis Date = 06/08/13 Pct Recovery = 78% Analysis Date = 06/08/13 Pct Recovery = 78% Analysis Date = 06/07/13 Pct Recovery = 79% Analysis Date = 06/07/13 Pct Recovery = 79% Analysis Date = 06/06/13 Pct Recovery = 80% Analysis Date = 06/06/13 Pct Recovery = 80% Analysis Date = 06/04/13 Pct Recovery = 80% Analysis Date = 06/04/13 Pct Recovery = 80% Analysis Date = 06/03/13 Pct Recovery = 81% Analysis Date = 06/03/13 Pct Recovery = 81% Analysis Date = 06/01/13 Pct Recovery = 82% Analysis Date = 06/01/13 Pct Recovery = 82% Analysis Date = 05/31/13 Pct Recovery = 82% Analysis Date = 05/31/13 Pct Recovery = 82% Analysis Date = 05/30/13 Pct Recovery = 83% Analysis Date = 05/30/13 Pct Recovery = 83% Analysis Date = 05/28/13 Pct Recovery = 82% Analysis Date = 05/28/13 Pct Recovery = 82% Analysis Date = 05/27/13 Pct Recovery = 81% Analysis Date = 05/27/13 Pct Recovery = 81% Analysis Date = 05/25/13 Pct Recovery = 81% Analysis Date = 05/25/13 Pct Recovery = 81% Analysis Date = 05/24/13 Pct Recovery = 81% Analysis Date = 05/24/13 Pct Recovery = 81% Analysis Date = 05/23/13 Pct Recovery = 80% Analysis Date = 05/23/13 Pct Recovery = 80% Analysis Date = 05/21/13 Pct Recovery = 80% Analysis Date = 05/21/13 Pct Recovery = 80% Analysis Date = 05/20/13 Pct Recovery = 80% Analysis Date = 05/20/13 Pct Recovery = 80% Analysis Date = 05/18/13 Pct Recovery = 80% Analysis Date = 05/18/13 Pct Recovery = 80% Analysis Date = 05/17/13 Pct Recovery = 79% Analysis Date = 05/17/13 Pct Recovery = 79% Analysis Date = 05/16/13 Pct Recovery = 79% Analysis Date = 05/16/13 Pct Recovery = 79% Analysis Date = 05/14/13 Pct Recovery = 79% Analysis Date = 05/14/13 Pct Recovery = 79% Analysis Date = 05/13/13 Pct Recovery = 78% Analysis Date = 05/13/13 Pct Recovery = 78% Analysis Date = 05/11/13 Pct Recovery = 78% Analysis Date = 05/11/13 Pct Recovery = 78% Analysis Date = 05/10/13 Pct Recovery = 78% Analysis Date = 05/10/13 Pct Recovery = 78% Analysis Date = 05/09/13 Pct Recovery = 78% Analysis Date = 05/09/13 Pct Recovery = 78% Analysis Date = 05/07/13 Pct Recovery = 77% Analysis Date = 05/07/13 Pct Recovery = 77% Analysis Date = 05/06/13 Pct Recovery = 77% Analysis Date = 05/06/13 Pct Recovery = 77% Analysis Date = 05/04/13 Pct Recovery = 77% Analysis Date = 05/04/13 Pct Recovery = 77% Analysis Date = 05/03/13 Pct Recovery = 76% Analysis Date = 05/03/13 Pct Recovery = 76% Analysis Date = 05/02/13 Pct Recovery = 76% Analysis Date = 05/02/13 Pct Recovery = 76% Analysis Date = 04/30/13 Pct Recovery = 76% Analysis Date = 04/30/13 Pct Recovery = 76% Analysis Date = 04/29/13 Pct Recovery = 76% Analysis Date = 04/29/13 Pct Recovery = 76% Analysis Date = 04/27/13 Pct Recovery = 75% Analysis Date = 04/27/13 Pct Recovery = 75% Analysis Date = 04/26/13 Pct Recovery = 75% Analysis Date = 04/26/13 Pct Recovery = 75% Analysis Date = 04/25/13 Pct Recovery = 75% Analysis Date = 04/25/13 Pct Recovery = 75% Analysis Date = 04/23/13 Pct Recovery = 74% Analysis Date = 04/23/13 Pct Recovery = 74% Analysis Date = 04/22/13 Pct Recovery = 74% Analysis Date = 04/22/13 Pct Recovery = 74% Analysis Date = 04/20/13 Pct Recovery = 74% Analysis Date = 04/20/13 Pct Recovery = 74% Analysis Date = 04/19/13 Pct Recovery = 74% Analysis Date = 04/19/13 Pct Recovery = 74% Analysis Date = 04/18/13 Pct Recovery = 73% Analysis Date = 04/18/13 Pct Recovery = 73% Analysis Date = 04/16/13 Pct Recovery = 73% Analysis Date = 04/16/13 Pct Recovery = 73% Analysis Date = 04/15/13 Pct Recovery = 73% Analysis Date = 04/15/13 Pct Recovery = 73% Analysis Date = 04/13/13 Pct Recovery = 72% Analysis Date = 04/13/13 Pct Recovery = 72% Analysis Date = 04/12/13 Pct Recovery = 72% Analysis Date = 04/12/13 Pct Recovery = 72% Analysis Date = 04/11/13 Pct Recovery = 72% Analysis Date = 04/11/13 Pct Recovery = 72% Analysis Date = 04/09/13 Pct Recovery = 72% Analysis Date = 04/09/13 Pct Recovery = 72% Analysis Date = 04/08/13 Pct Recovery = 71% Analysis Date = 04/08/13 Pct Recovery = 71% Analysis Date = 04/06/13 Pct Recovery = 71% Analysis Date = 04/06/13 Pct Recovery = 71% Analysis Date = 04/05/13 Pct Recovery = 71% Analysis Date = 04/05/13 Pct Recovery = 71% Analysis Date = 04/04/13 Pct Recovery = 70% Analysis Date = 04/04/13 Pct Recovery = 70% Analysis Date = 04/02/13 Pct Recovery = 70% Analysis Date = 04/02/13 Pct Recovery = 70% Analysis Date = 04/01/13 Pct Recovery = 70% Analysis Date = 04/01/13 Pct Recovery = 70% Analysis Date = 03/30/13 Pct Recovery = 70% Analysis Date = 03/30/13 Pct Recovery = 70% Analysis Date = 03/29/13 Pct Recovery = 69% Analysis Date = 03/29/13 Pct Recovery = 69% Analysis Date = 03/28/13 Pct Recovery = 69% Analysis Date = 03/28/13 Pct Recovery = 69% Analysis Date = 03/26/13 Pct Recovery = 69% Analysis Date = 03/26/13 Pct Recovery = 69% Analysis Date = 03/25/13 Pct Recovery = 69% Analysis Date = 03/25/13 Pct Recovery = 69% Analysis Date = 03/23/13 Pct Recovery = 69% Analysis Date = 03/23/13 Pct Recovery = 69% Analysis Date = 03/22/13 Pct Recovery = 69% Analysis Date = 03/22/13 Pct Recovery = 69% Analysis Date = 03/21/13 Pct Recovery = 69% Analysis Date = 03/21/13 Pct Recovery = 69% Analysis Date = 03/19/13 Pct Recovery = 70% Analysis Date = 03/19/13 Pct Recovery = 70% Analysis Date = 03/18/13 Pct Recovery = 70% Analysis Date = 03/18/13 Pct Recovery = 70% Analysis Date = 03/16/13 Pct Recovery = 70% Analysis Date = 03/16/13 Pct Recovery = 70% Analysis Date = 03/15/13 Pct Recovery = 70% Analysis Date = 03/15/13 Pct Recovery = 70% Analysis Date = 03/14/13 Pct Recovery = 70% Analysis Date = 03/14/13 Pct Recovery = 70% Analysis Date = 03/12/13 Pct Recovery = 70% Analysis Date = 03/12/13 Pct Recovery = 70% Analysis Date = 03/11/13 Pct Recovery = 70% Analysis Date = 03/11/13 Pct Recovery = 70% Analysis Date = 03/09/13 Pct Recovery = 71% Analysis Date = 03/09/13 Pct Recovery = 71% Analysis Date = 03/08/13 Pct Recovery = 71% Analysis Date = 03/08/13 Pct Recovery = 71% Analysis Date = 03/07/13 Pct Recovery = 71% Analysis Date = 03/07/13 Pct Recovery = 71% Analysis Date = 03/05/13 Pct Recovery = 71% Analysis Date = 03/05/13 Pct Recovery = 71% Analysis Date = 03/04/13 Pct Recovery = 71% Analysis Date = 03/04/13 Pct Recovery = 71% Analysis Date = 03/02/13 Pct Recovery = 71% Analysis Date = 03/02/13 Pct Recovery = 71% Analysis Date = 03/01/13 Pct Recovery = 71% Analysis Date = 03/01/13 Pct Recovery = 71% Analysis Date = 02/28/13 Pct Recovery = 72% Analysis Date = 02/28/13 Pct Recovery = 72% Analysis Date = 02/26/13 Pct Recovery = 72% Analysis Date = 02/26/13 Pct Recovery = 72% Analysis Date = 02/25/13 Pct Recovery = 72% Analysis Date = 02/25/13 Pct Recovery = 72% Analysis Date = 02/23/13 Pct Recovery = 72% Analysis Date = 02/23/13 Pct Recovery = 72% Analysis Date = 02/22/13 Pct Recovery = 72% Analysis Date = 02/22/13 Pct Recovery = 72% Analysis Date = 02/21/13 Pct Recovery = 72% Analysis Date = 02/21/13 Pct Recovery = 72% Analysis Date = 02/19/13 Pct Recovery = 72% Analysis Date = 02/19/13 Pct Recovery = 72% Analysis Date = 02/18/13 Pct Recovery = 72% Analysis Date = 02/18/13 Pct Recovery = 72% Analysis Date = 02/16/13 Pct Recovery = 73% Analysis Date = 02/16/13 Pct Recovery = 73% Analysis Date = 02/15/13 Pct Recovery = 73% Analysis Date = 02/15/13 Pct Recovery = 73% Analysis Date = 02/14/13 Pct Recovery = 73% Analysis Date = 02/14/13 Pct Recovery = 73% Analysis Date = 02/12/13 Pct Recovery = 73% Analysis Date = 02/12/13 Pct Recovery = 73% Analysis Date = 02/11/13 Pct Recovery = 73% Analysis Date = 02/11/13 Pct Recovery = 73% Analysis Date = 02/09/13 Pct Recovery = 73% Analysis Date = 02/09/13 Pct Recovery = 73% Analysis Date = 02/08/13 Pct Recovery = 73% Analysis Date = 02/08/13 Pct Recovery = 73% Analysis Date = 02/07/13 Pct Recovery = 74% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
ISOQUINOLINE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 8 83% 16% 77% 18%
Total 8 83% 16% 77% 18%

Sample Statistics
ISOQUINOLINE

Characteristic N % % Basis
Plotted 8 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 8 .  
False Negatives 0 0% 0 out of 8
Not Spiked 7 .  
False Positives 0 0% 0 out of 7