OBSP Determination:
1-NAPHTHOL
METHOD: 2033 , TESTIDCODE: 49295GCM39

Laboratory ID = 20140100085 Lab Value = 0.106 Expected Conc. = 0.451 Report level label = 0.05 Pct Recovery = 24% Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl SpecificMix = 042413 Laboratory ID = 20163370001 Lab Value = 0.183 Expected Conc. = 0.314 Report level label = 0.05 Pct Recovery = 58% Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl SpecificMix = B20160331 Laboratory ID = 20163150006 Lab Value = 0.132 Expected Conc. = 0.314 Report level label = 0.05 Pct Recovery = 42% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl SpecificMix = B20160331 Laboratory ID = 20161880109 Lab Value = 0.204 Expected Conc. = 0.313 Report level label = 0.05 Pct Recovery = 65% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl SpecificMix = 03FF076 Laboratory ID = 20152750006 Lab Value = 0.071 Expected Conc. = 0.3 Report level label = 0.05 Pct Recovery = 24% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl SpecificMix = EN150514012 Laboratory ID = 20152460215 Lab Value = 0.110 Expected Conc. = 0.3 Report level label = 0.05 Pct Recovery = 37% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl SpecificMix = EN150514012 Laboratory ID = 20171720140 Lab Value = 0.088 Expected Conc. = 0.2512 Report level label = 0.05 Pct Recovery = 35% Analysis Date = 08/31/17 SpikeMix = Supelco LC20138V: 80 µl & Phenova B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20171660002 Lab Value = 0.205 Expected Conc. = 0.2512 Report level label = 0.05 Pct Recovery = 82% Analysis Date = 08/23/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20170190026 Lab Value = 0.129 Expected Conc. = 0.2512 Report level label = 0.05 Pct Recovery = 51% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20161470001 Lab Value = 0.140 Expected Conc. = 0.2512 Report level label = 0.05 Pct Recovery = 56% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20170960001 Lab Value = 0.126 Expected Conc. = 0.2504 Report level label = 0.05 Pct Recovery = 50% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl SpecificMix = 03FF076 Laboratory ID = 20132690010 Lab Value = 0.150 Expected Conc. = 0.2255 Report level label = 0.05 Pct Recovery = 67% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl SpecificMix = 042413 Laboratory ID = 20132560001 Lab Value = 0.134 Expected Conc. = 0.2255 Report level label = 0.05 Pct Recovery = 59% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl SpecificMix = 042413 Laboratory ID = 20132140002 Lab Value = 0.121 Expected Conc. = 0.225 Report level label = 0.05 Pct Recovery = 54% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl SpecificMix = 04CC101 Laboratory ID = 20130250061 Lab Value = 0.083 Expected Conc. = 0.2 Report level label = 0.05 Pct Recovery = 41% Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl SpecificMix = 05BB029 Laboratory ID = 20150430092 Lab Value = 0.026 Expected Conc. = 0.1998 Report level label = 0.05 Pct Recovery = 13% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl SpecificMix = 042814 Laboratory ID = 20143240095 Lab Value = 0.064 Expected Conc. = 0.1998 Report level label = 0.05 Pct Recovery = 32% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl SpecificMix = 042814 Laboratory ID = 20142960086 Lab Value = 0.099 Expected Conc. = 0.1998 Report level label = 0.05 Pct Recovery = 50% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 042814 Laboratory ID = 20142530087 Lab Value = 0.048 Expected Conc. = 0.1998 Report level label = 0.05 Pct Recovery = 24% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl SpecificMix = 042814 Laboratory ID = 20150720069 Lab Value = 0.031 Expected Conc. = 0.1992 Report level label = 0.05 Pct Recovery = 15% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 0227-14-08 Laboratory ID = 20141770149 Lab Value = 0.077 Expected Conc. = 0.1992 Report level label = 0.05 Pct Recovery = 39% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl SpecificMix = 0227-14-08 Laboratory ID = 20141570088 Lab Value = 0.087 Expected Conc. = 0.1992 Report level label = 0.05 Pct Recovery = 44% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl SpecificMix = 0227-14-08 Laboratory ID = 20172230001 Lab Value = 0.115 Expected Conc. = 0.165 Report level label = 0.05 Pct Recovery = 70% Analysis Date = 10/19/17 SpikeMix = ChemService 6472100: 50 µl & Abs 071717Pest: 50 µl SpecificMix = 6472100 Laboratory ID = 20160630046 Lab Value = 0.038 Expected Conc. = 0.15 Report level label = 0.05 Pct Recovery = 25% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = EN150514012 Laboratory ID = 20153440001 Lab Value = 0.057 Expected Conc. = 0.15 Report level label = 0.05 Pct Recovery = 38% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = EN150514012 Laboratory ID = 20152330039 Lab Value = 0.063 Expected Conc. = 0.1484 Report level label = 0.05 Pct Recovery = 42% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl SpecificMix = 041415 Laboratory ID = 20151900132 Lab Value = 0.042 Expected Conc. = 0.1484 Report level label = 0.05 Pct Recovery = 29% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl SpecificMix = 041415 Laboratory ID = 20151270112 Lab Value = 0.091 Expected Conc. = 0.1484 Report level label = 0.05 Pct Recovery = 62% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl SpecificMix = 041415 Laboratory ID = 20171160110 Lab Value = 0.106 Expected Conc. = 0.1256 Report level label = 0.05 Pct Recovery = 84% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = B20160331 Laboratory ID = 20162380004 Lab Value = 0.061 Expected Conc. = 0.1256 Report level label = 0.05 Pct Recovery = 49% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = B20160331 Laboratory ID = 20162150213 Lab Value = 0.078 Expected Conc. = 0.1256 Report level label = 0.05 Pct Recovery = 62% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl SpecificMix = B20160331 Laboratory ID = 20172020035 Lab Value = 0.078 Expected Conc. = 0.1252 Report level label = 0.05 Pct Recovery = 62% Analysis Date = 11/07/17 SpikeMix = Abs 071717Pest: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20171510080 Lab Value = 0.067 Expected Conc. = 0.1252 Report level label = 0.05 Pct Recovery = 54% Analysis Date = 06/09/17 SpikeMix = Supelco LC20138V: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20170460061 Lab Value = 0.067 Expected Conc. = 0.1252 Report level label = 0.05 Pct Recovery = 54% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl SpecificMix = 03FF076 Laboratory ID = 20162660005 Lab Value = 0.069 Expected Conc. = 0.1252 Report level label = 0.05 Pct Recovery = 55% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl SpecificMix = 03FF076 Laboratory ID = 20161600087 Lab Value = 0.089 Expected Conc. = 0.1252 Report level label = 0.05 Pct Recovery = 71% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20161340228 Lab Value = 0.041 Expected Conc. = 0.1252 Report level label = 0.05 Pct Recovery = 33% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl SpecificMix = 03FF076 Laboratory ID = 20161190075 Lab Value = 0.041 Expected Conc. = 0.1252 Report level label = 0.05 Pct Recovery = 33% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20140230082 Lab Value = 0.041 Expected Conc. = 0.101 Report level label = 0.05 Pct Recovery = 40% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl SpecificMix = 012513 Laboratory ID = 20132420001 Lab Value = 0.081 Expected Conc. = 0.101 Report level label = 0.05 Pct Recovery = 80% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl SpecificMix = 012513 Laboratory ID = 20130940097 Lab Value = 0.051 Expected Conc. = 0.101 Report level label = 0.05 Pct Recovery = 50% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = 052412 Laboratory ID = 20130100066 Lab Value = 0.045 Expected Conc. = 0.101 Report level label = 0.05 Pct Recovery = 44% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl SpecificMix = 052412 Laboratory ID = 20143370094 Lab Value = 0.014 Expected Conc. = 0.0999 Report level label = 0.05 Pct Recovery = 14% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl SpecificMix = 042814 Laboratory ID = 20142820151 Lab Value = 0.039 Expected Conc. = 0.0999 Report level label = 0.05 Pct Recovery = 39% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl SpecificMix = 042814 Laboratory ID = 20142470041 Lab Value = 0.020 Expected Conc. = 0.0999 Report level label = 0.05 Pct Recovery = 20% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl SpecificMix = 042814 Laboratory ID = 20142200164 Lab Value = 0.063 Expected Conc. = 0.0999 Report level label = 0.05 Pct Recovery = 63% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 042814 Laboratory ID = 20141840097 Lab Value = 0.021 Expected Conc. = 0.0996 Report level label = 0.05 Pct Recovery = 21% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20141490205 Lab Value = 0.073 Expected Conc. = 0.0996 Report level label = 0.05 Pct Recovery = 73% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20141420140 Lab Value = 0.026 Expected Conc. = 0.0996 Report level label = 0.05 Pct Recovery = 26% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20141360094 Lab Value = 0.043 Expected Conc. = 0.0996 Report level label = 0.05 Pct Recovery = 43% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20173120093 Lab Value = 0.034 Expected Conc. = 0.099 Report level label = 0.05 Pct Recovery = 34% Analysis Date = 03/10/18 SpikeMix = ChemService 6472100: 30 µl & ChemService 6537100: 30 µl SpecificMix = 6472100 Laboratory ID = 20133580036 Lab Value = 0.016 Expected Conc. = 0.0902 Report level label = 0.05 Pct Recovery = 17% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 042413 Laboratory ID = 20133190012 Lab Value = 0.053 Expected Conc. = 0.0902 Report level label = 0.05 Pct Recovery = 58% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 042413 Laboratory ID = 20131650073 Lab Value = 0.035 Expected Conc. = 0.0902 Report level label = 0.05 Pct Recovery = 39% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl SpecificMix = 042413 Laboratory ID = 20140730138 Lab Value = 0.017 Expected Conc. = 0.09 Report level label = 0.05 Pct Recovery = 18% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 04CC101 Laboratory ID = 20140510043 Lab Value = 0.028 Expected Conc. = 0.09 Report level label = 0.05 Pct Recovery = 31% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 04CC101 Laboratory ID = 20133310030 Lab Value = 0.060 Expected Conc. = 0.09 Report level label = 0.05 Pct Recovery = 66% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl SpecificMix = 04CC101 Laboratory ID = 20132280016 Lab Value = 0.069 Expected Conc. = 0.09 Report level label = 0.05 Pct Recovery = 76% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl SpecificMix = 04CC101 Laboratory ID = 20131510026 Lab Value = 0.025 Expected Conc. = 0.09 Report level label = 0.05 Pct Recovery = 28% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl SpecificMix = 04CC101 Laboratory ID = 20160070059 Lab Value = 0.037 Expected Conc. = 0.075 Report level label = 0.05 Pct Recovery = 50% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = EN150514012 Laboratory ID = 20153160001 Lab Value = 0.038 Expected Conc. = 0.075 Report level label = 0.05 Pct Recovery = 50% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = EN150514012 Laboratory ID = 20151760208 Lab Value = 0.010 Expected Conc. = 0.075 Report level label = 0.05 Pct Recovery = 13% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl SpecificMix = EN150514012 Laboratory ID = 20151480170 Lab Value = 0.035 Expected Conc. = 0.075 Report level label = 0.05 Pct Recovery = 47% Analysis Date = 06/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150514012 Laboratory ID = 20161050143 Lab Value = 0.027 Expected Conc. = 0.0742 Report level label = 0.05 Pct Recovery = 36% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 041415 Laboratory ID = 20160560044 Lab Value = 0.018 Expected Conc. = 0.0742 Report level label = 0.05 Pct Recovery = 24% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl SpecificMix = 041415 Laboratory ID = 20160210080 Lab Value = 0.027 Expected Conc. = 0.0742 Report level label = 0.05 Pct Recovery = 36% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 041415 Laboratory ID = 20152950078 Lab Value = 0.014 Expected Conc. = 0.0742 Report level label = 0.05 Pct Recovery = 19% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 041415 Laboratory ID = 20152040177 Lab Value = 0.029 Expected Conc. = 0.0742 Report level label = 0.05 Pct Recovery = 39% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl SpecificMix = 041415 Laboratory ID = 20151210037 Lab Value = 0.030 Expected Conc. = 0.0742 Report level label = 0.05 Pct Recovery = 40% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 041415 Laboratory ID = 20140860102 Lab Value = 0.012 Expected Conc. = 0.0404 Report level label = 0.05 Pct Recovery = 29% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 012513 Laboratory ID = 20133400002 Lab Value = 0.023 Expected Conc. = 0.0404 Report level label = 0.05 Pct Recovery = 56% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = 052412 Laboratory ID = 20132910008 Lab Value = 0.024 Expected Conc. = 0.0404 Report level label = 0.05 Pct Recovery = 60% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = 052412 Laboratory ID = 20131920149 Lab Value = 0.015 Expected Conc. = 0.0404 Report level label = 0.05 Pct Recovery = 38% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl SpecificMix = 012513 Laboratory ID = 20130650005 Lab Value = 0.017 Expected Conc. = 0.0404 Report level label = 0.05 Pct Recovery = 41% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl SpecificMix = 052412 Laboratory ID = 20131230084 Lab Value = 0.023 Expected Conc. = 0.04 Report level label = 0.05 Pct Recovery = 59% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl SpecificMix = 05BB029 Laboratory ID = 20130510051 Lab Value = 0.014 Expected Conc. = 0.04 Report level label = 0.05 Pct Recovery = 36% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl SpecificMix = 05BB029 Analysis Date = 03/09/18 Pct Recovery = 64% Analysis Date = 02/28/18 Pct Recovery = 64% Analysis Date = 02/28/18 Pct Recovery = 64% Analysis Date = 02/19/18 Pct Recovery = 64% Analysis Date = 02/19/18 Pct Recovery = 64% Analysis Date = 02/09/18 Pct Recovery = 63% Analysis Date = 02/09/18 Pct Recovery = 63% Analysis Date = 01/31/18 Pct Recovery = 63% Analysis Date = 01/31/18 Pct Recovery = 63% Analysis Date = 01/22/18 Pct Recovery = 63% Analysis Date = 01/22/18 Pct Recovery = 63% Analysis Date = 01/12/18 Pct Recovery = 62% Analysis Date = 01/12/18 Pct Recovery = 62% Analysis Date = 01/03/18 Pct Recovery = 62% Analysis Date = 01/03/18 Pct Recovery = 62% Analysis Date = 12/24/17 Pct Recovery = 62% Analysis Date = 12/24/17 Pct Recovery = 62% Analysis Date = 12/15/17 Pct Recovery = 62% Analysis Date = 12/15/17 Pct Recovery = 62% Analysis Date = 12/06/17 Pct Recovery = 61% Analysis Date = 12/06/17 Pct Recovery = 61% Analysis Date = 11/26/17 Pct Recovery = 61% Analysis Date = 11/26/17 Pct Recovery = 61% Analysis Date = 11/17/17 Pct Recovery = 61% Analysis Date = 11/17/17 Pct Recovery = 61% Analysis Date = 11/07/17 Pct Recovery = 61% Analysis Date = 11/07/17 Pct Recovery = 61% Analysis Date = 10/29/17 Pct Recovery = 60% Analysis Date = 10/29/17 Pct Recovery = 60% Analysis Date = 10/20/17 Pct Recovery = 60% Analysis Date = 10/20/17 Pct Recovery = 60% Analysis Date = 10/10/17 Pct Recovery = 60% Analysis Date = 10/10/17 Pct Recovery = 60% Analysis Date = 10/01/17 Pct Recovery = 59% Analysis Date = 10/01/17 Pct Recovery = 59% Analysis Date = 09/21/17 Pct Recovery = 59% Analysis Date = 09/21/17 Pct Recovery = 59% Analysis Date = 09/12/17 Pct Recovery = 59% Analysis Date = 09/12/17 Pct Recovery = 59% Analysis Date = 09/03/17 Pct Recovery = 59% Analysis Date = 09/03/17 Pct Recovery = 59% Analysis Date = 08/24/17 Pct Recovery = 58% Analysis Date = 08/24/17 Pct Recovery = 58% Analysis Date = 08/15/17 Pct Recovery = 58% Analysis Date = 08/15/17 Pct Recovery = 58% Analysis Date = 08/06/17 Pct Recovery = 58% Analysis Date = 08/06/17 Pct Recovery = 58% Analysis Date = 07/27/17 Pct Recovery = 57% Analysis Date = 07/27/17 Pct Recovery = 57% Analysis Date = 07/18/17 Pct Recovery = 57% Analysis Date = 07/18/17 Pct Recovery = 57% Analysis Date = 07/08/17 Pct Recovery = 57% Analysis Date = 07/08/17 Pct Recovery = 57% Analysis Date = 06/29/17 Pct Recovery = 57% Analysis Date = 06/29/17 Pct Recovery = 57% Analysis Date = 06/20/17 Pct Recovery = 56% Analysis Date = 06/20/17 Pct Recovery = 56% Analysis Date = 06/10/17 Pct Recovery = 56% Analysis Date = 06/10/17 Pct Recovery = 56% Analysis Date = 06/01/17 Pct Recovery = 56% Analysis Date = 06/01/17 Pct Recovery = 56% Analysis Date = 05/22/17 Pct Recovery = 56% Analysis Date = 05/22/17 Pct Recovery = 56% Analysis Date = 05/13/17 Pct Recovery = 55% Analysis Date = 05/13/17 Pct Recovery = 55% Analysis Date = 05/04/17 Pct Recovery = 55% Analysis Date = 05/04/17 Pct Recovery = 55% Analysis Date = 04/24/17 Pct Recovery = 55% Analysis Date = 04/24/17 Pct Recovery = 55% Analysis Date = 04/15/17 Pct Recovery = 54% Analysis Date = 04/15/17 Pct Recovery = 54% Analysis Date = 04/05/17 Pct Recovery = 54% Analysis Date = 04/05/17 Pct Recovery = 54% Analysis Date = 03/27/17 Pct Recovery = 54% Analysis Date = 03/27/17 Pct Recovery = 54% Analysis Date = 03/18/17 Pct Recovery = 54% Analysis Date = 03/18/17 Pct Recovery = 54% Analysis Date = 03/08/17 Pct Recovery = 53% Analysis Date = 03/08/17 Pct Recovery = 53% Analysis Date = 02/27/17 Pct Recovery = 53% Analysis Date = 02/27/17 Pct Recovery = 53% Analysis Date = 02/18/17 Pct Recovery = 53% Analysis Date = 02/18/17 Pct Recovery = 53% Analysis Date = 02/08/17 Pct Recovery = 52% Analysis Date = 02/08/17 Pct Recovery = 52% Analysis Date = 01/30/17 Pct Recovery = 52% Analysis Date = 01/30/17 Pct Recovery = 52% Analysis Date = 01/20/17 Pct Recovery = 52% Analysis Date = 01/20/17 Pct Recovery = 52% Analysis Date = 01/11/17 Pct Recovery = 52% Analysis Date = 01/11/17 Pct Recovery = 52% Analysis Date = 01/02/17 Pct Recovery = 51% Analysis Date = 01/02/17 Pct Recovery = 51% Analysis Date = 12/23/16 Pct Recovery = 51% Analysis Date = 12/23/16 Pct Recovery = 51% Analysis Date = 12/14/16 Pct Recovery = 51% Analysis Date = 12/14/16 Pct Recovery = 51% Analysis Date = 12/04/16 Pct Recovery = 50% Analysis Date = 12/04/16 Pct Recovery = 50% Analysis Date = 11/25/16 Pct Recovery = 50% Analysis Date = 11/25/16 Pct Recovery = 50% Analysis Date = 11/16/16 Pct Recovery = 50% Analysis Date = 11/16/16 Pct Recovery = 50% Analysis Date = 11/06/16 Pct Recovery = 50% Analysis Date = 11/06/16 Pct Recovery = 50% Analysis Date = 10/28/16 Pct Recovery = 49% Analysis Date = 10/28/16 Pct Recovery = 49% Analysis Date = 10/18/16 Pct Recovery = 49% Analysis Date = 10/18/16 Pct Recovery = 49% Analysis Date = 10/09/16 Pct Recovery = 49% Analysis Date = 10/09/16 Pct Recovery = 49% Analysis Date = 09/30/16 Pct Recovery = 48% Analysis Date = 09/30/16 Pct Recovery = 48% Analysis Date = 09/20/16 Pct Recovery = 48% Analysis Date = 09/20/16 Pct Recovery = 48% Analysis Date = 09/11/16 Pct Recovery = 48% Analysis Date = 09/11/16 Pct Recovery = 48% Analysis Date = 09/01/16 Pct Recovery = 47% Analysis Date = 09/01/16 Pct Recovery = 47% Analysis Date = 08/23/16 Pct Recovery = 47% Analysis Date = 08/23/16 Pct Recovery = 47% Analysis Date = 08/14/16 Pct Recovery = 47% Analysis Date = 08/14/16 Pct Recovery = 47% Analysis Date = 08/04/16 Pct Recovery = 46% Analysis Date = 08/04/16 Pct Recovery = 46% Analysis Date = 07/26/16 Pct Recovery = 46% Analysis Date = 07/26/16 Pct Recovery = 46% Analysis Date = 07/17/16 Pct Recovery = 46% Analysis Date = 07/17/16 Pct Recovery = 46% Analysis Date = 07/07/16 Pct Recovery = 45% Analysis Date = 07/07/16 Pct Recovery = 45% Analysis Date = 06/28/16 Pct Recovery = 45% Analysis Date = 06/28/16 Pct Recovery = 45% Analysis Date = 06/18/16 Pct Recovery = 45% Analysis Date = 06/18/16 Pct Recovery = 45% Analysis Date = 06/09/16 Pct Recovery = 44% Analysis Date = 06/09/16 Pct Recovery = 44% Analysis Date = 05/31/16 Pct Recovery = 44% Analysis Date = 05/31/16 Pct Recovery = 44% Analysis Date = 05/21/16 Pct Recovery = 44% Analysis Date = 05/21/16 Pct Recovery = 44% Analysis Date = 05/12/16 Pct Recovery = 43% Analysis Date = 05/12/16 Pct Recovery = 43% Analysis Date = 05/02/16 Pct Recovery = 43% Analysis Date = 05/02/16 Pct Recovery = 43% Analysis Date = 04/23/16 Pct Recovery = 43% Analysis Date = 04/23/16 Pct Recovery = 43% Analysis Date = 04/14/16 Pct Recovery = 42% Analysis Date = 04/14/16 Pct Recovery = 42% Analysis Date = 04/04/16 Pct Recovery = 42% Analysis Date = 04/04/16 Pct Recovery = 42% Analysis Date = 03/26/16 Pct Recovery = 42% Analysis Date = 03/26/16 Pct Recovery = 42% Analysis Date = 03/16/16 Pct Recovery = 41% Analysis Date = 03/16/16 Pct Recovery = 41% Analysis Date = 03/07/16 Pct Recovery = 41% Analysis Date = 03/07/16 Pct Recovery = 41% Analysis Date = 02/27/16 Pct Recovery = 40% Analysis Date = 02/27/16 Pct Recovery = 40% Analysis Date = 02/17/16 Pct Recovery = 40% Analysis Date = 02/17/16 Pct Recovery = 40% Analysis Date = 02/08/16 Pct Recovery = 40% Analysis Date = 02/08/16 Pct Recovery = 40% Analysis Date = 01/30/16 Pct Recovery = 39% Analysis Date = 01/30/16 Pct Recovery = 39% Analysis Date = 01/20/16 Pct Recovery = 39% Analysis Date = 01/20/16 Pct Recovery = 39% Analysis Date = 01/11/16 Pct Recovery = 39% Analysis Date = 01/11/16 Pct Recovery = 39% Analysis Date = 01/01/16 Pct Recovery = 39% Analysis Date = 01/01/16 Pct Recovery = 39% Analysis Date = 12/23/15 Pct Recovery = 38% Analysis Date = 12/23/15 Pct Recovery = 38% Analysis Date = 12/14/15 Pct Recovery = 38% Analysis Date = 12/14/15 Pct Recovery = 38% Analysis Date = 12/04/15 Pct Recovery = 38% Analysis Date = 12/04/15 Pct Recovery = 38% Analysis Date = 11/25/15 Pct Recovery = 38% Analysis Date = 11/25/15 Pct Recovery = 38% Analysis Date = 11/15/15 Pct Recovery = 38% Analysis Date = 11/15/15 Pct Recovery = 38% Analysis Date = 11/06/15 Pct Recovery = 37% Analysis Date = 11/06/15 Pct Recovery = 37% Analysis Date = 10/28/15 Pct Recovery = 37% Analysis Date = 10/28/15 Pct Recovery = 37% Analysis Date = 10/18/15 Pct Recovery = 37% Analysis Date = 10/18/15 Pct Recovery = 37% Analysis Date = 10/09/15 Pct Recovery = 37% Analysis Date = 10/09/15 Pct Recovery = 37% Analysis Date = 09/29/15 Pct Recovery = 36% Analysis Date = 09/29/15 Pct Recovery = 36% Analysis Date = 09/20/15 Pct Recovery = 36% Analysis Date = 09/20/15 Pct Recovery = 36% Analysis Date = 09/11/15 Pct Recovery = 36% Analysis Date = 09/11/15 Pct Recovery = 36% Analysis Date = 09/01/15 Pct Recovery = 36% Analysis Date = 09/01/15 Pct Recovery = 36% Analysis Date = 08/23/15 Pct Recovery = 36% Analysis Date = 08/23/15 Pct Recovery = 36% Analysis Date = 08/13/15 Pct Recovery = 35% Analysis Date = 08/13/15 Pct Recovery = 35% Analysis Date = 08/04/15 Pct Recovery = 35% Analysis Date = 08/04/15 Pct Recovery = 35% Analysis Date = 07/26/15 Pct Recovery = 35% Analysis Date = 07/26/15 Pct Recovery = 35% Analysis Date = 07/16/15 Pct Recovery = 35% Analysis Date = 07/16/15 Pct Recovery = 35% Analysis Date = 07/07/15 Pct Recovery = 35% Analysis Date = 07/07/15 Pct Recovery = 35% Analysis Date = 06/28/15 Pct Recovery = 35% Analysis Date = 06/28/15 Pct Recovery = 35% Analysis Date = 06/18/15 Pct Recovery = 35% Analysis Date = 06/18/15 Pct Recovery = 35% Analysis Date = 06/09/15 Pct Recovery = 35% Analysis Date = 06/09/15 Pct Recovery = 35% Analysis Date = 05/30/15 Pct Recovery = 35% Analysis Date = 05/30/15 Pct Recovery = 35% Analysis Date = 05/21/15 Pct Recovery = 35% Analysis Date = 05/21/15 Pct Recovery = 35% Analysis Date = 05/12/15 Pct Recovery = 35% Analysis Date = 05/12/15 Pct Recovery = 35% Analysis Date = 05/02/15 Pct Recovery = 35% Analysis Date = 05/02/15 Pct Recovery = 35% Analysis Date = 04/23/15 Pct Recovery = 35% Analysis Date = 04/23/15 Pct Recovery = 35% Analysis Date = 04/13/15 Pct Recovery = 35% Analysis Date = 04/13/15 Pct Recovery = 35% Analysis Date = 04/04/15 Pct Recovery = 34% Analysis Date = 04/04/15 Pct Recovery = 34% Analysis Date = 03/26/15 Pct Recovery = 34% Analysis Date = 03/26/15 Pct Recovery = 34% Analysis Date = 03/16/15 Pct Recovery = 34% Analysis Date = 03/16/15 Pct Recovery = 34% Analysis Date = 03/07/15 Pct Recovery = 34% Analysis Date = 03/07/15 Pct Recovery = 34% Analysis Date = 02/25/15 Pct Recovery = 34% Analysis Date = 02/25/15 Pct Recovery = 34% Analysis Date = 02/16/15 Pct Recovery = 35% Analysis Date = 02/16/15 Pct Recovery = 35% Analysis Date = 02/07/15 Pct Recovery = 35% Analysis Date = 02/07/15 Pct Recovery = 35% Analysis Date = 01/28/15 Pct Recovery = 35% Analysis Date = 01/28/15 Pct Recovery = 35% Analysis Date = 01/19/15 Pct Recovery = 35% Analysis Date = 01/19/15 Pct Recovery = 35% Analysis Date = 01/10/15 Pct Recovery = 35% Analysis Date = 01/10/15 Pct Recovery = 35% Analysis Date = 12/31/14 Pct Recovery = 35% Analysis Date = 12/31/14 Pct Recovery = 35% Analysis Date = 12/22/14 Pct Recovery = 35% Analysis Date = 12/22/14 Pct Recovery = 35% Analysis Date = 12/12/14 Pct Recovery = 36% Analysis Date = 12/12/14 Pct Recovery = 36% Analysis Date = 12/03/14 Pct Recovery = 36% Analysis Date = 12/03/14 Pct Recovery = 36% Analysis Date = 11/24/14 Pct Recovery = 36% Analysis Date = 11/24/14 Pct Recovery = 36% Analysis Date = 11/14/14 Pct Recovery = 36% Analysis Date = 11/14/14 Pct Recovery = 36% Analysis Date = 11/05/14 Pct Recovery = 36% Analysis Date = 11/05/14 Pct Recovery = 36% Analysis Date = 10/26/14 Pct Recovery = 36% Analysis Date = 10/26/14 Pct Recovery = 36% Analysis Date = 10/17/14 Pct Recovery = 37% Analysis Date = 10/17/14 Pct Recovery = 37% Analysis Date = 10/08/14 Pct Recovery = 37% Analysis Date = 10/08/14 Pct Recovery = 37% Analysis Date = 09/28/14 Pct Recovery = 37% Analysis Date = 09/28/14 Pct Recovery = 37% Analysis Date = 09/19/14 Pct Recovery = 37% Analysis Date = 09/19/14 Pct Recovery = 37% Analysis Date = 09/09/14 Pct Recovery = 37% Analysis Date = 09/09/14 Pct Recovery = 37% Analysis Date = 08/31/14 Pct Recovery = 37% Analysis Date = 08/31/14 Pct Recovery = 37% Analysis Date = 08/22/14 Pct Recovery = 38% Analysis Date = 08/22/14 Pct Recovery = 38% Analysis Date = 08/12/14 Pct Recovery = 38% Analysis Date = 08/12/14 Pct Recovery = 38% Analysis Date = 08/03/14 Pct Recovery = 38% Analysis Date = 08/03/14 Pct Recovery = 38% Analysis Date = 07/25/14 Pct Recovery = 38% Analysis Date = 07/25/14 Pct Recovery = 38% Analysis Date = 07/15/14 Pct Recovery = 38% Analysis Date = 07/15/14 Pct Recovery = 38% Analysis Date = 07/06/14 Pct Recovery = 38% Analysis Date = 07/06/14 Pct Recovery = 38% Analysis Date = 06/26/14 Pct Recovery = 39% Analysis Date = 06/26/14 Pct Recovery = 39% Analysis Date = 06/17/14 Pct Recovery = 39% Analysis Date = 06/17/14 Pct Recovery = 39% Analysis Date = 06/08/14 Pct Recovery = 39% Analysis Date = 06/08/14 Pct Recovery = 39% Analysis Date = 05/29/14 Pct Recovery = 40% Analysis Date = 05/29/14 Pct Recovery = 40% Analysis Date = 05/20/14 Pct Recovery = 40% Analysis Date = 05/20/14 Pct Recovery = 40% Analysis Date = 05/10/14 Pct Recovery = 40% Analysis Date = 05/10/14 Pct Recovery = 40% Analysis Date = 05/01/14 Pct Recovery = 41% Analysis Date = 05/01/14 Pct Recovery = 41% Analysis Date = 04/22/14 Pct Recovery = 41% Analysis Date = 04/22/14 Pct Recovery = 41% Analysis Date = 04/12/14 Pct Recovery = 42% Analysis Date = 04/12/14 Pct Recovery = 42% Analysis Date = 04/03/14 Pct Recovery = 42% Analysis Date = 04/03/14 Pct Recovery = 42% Analysis Date = 03/24/14 Pct Recovery = 42% Analysis Date = 03/24/14 Pct Recovery = 42% Analysis Date = 03/15/14 Pct Recovery = 42% Analysis Date = 03/15/14 Pct Recovery = 42% Analysis Date = 03/06/14 Pct Recovery = 43% Analysis Date = 03/06/14 Pct Recovery = 43% Analysis Date = 02/24/14 Pct Recovery = 43% Analysis Date = 02/24/14 Pct Recovery = 43% Analysis Date = 02/15/14 Pct Recovery = 43% Analysis Date = 02/15/14 Pct Recovery = 43% Analysis Date = 02/05/14 Pct Recovery = 43% Analysis Date = 02/05/14 Pct Recovery = 43% Analysis Date = 01/27/14 Pct Recovery = 44% Analysis Date = 01/27/14 Pct Recovery = 44% Analysis Date = 01/18/14 Pct Recovery = 44% Analysis Date = 01/18/14 Pct Recovery = 44% Analysis Date = 01/08/14 Pct Recovery = 44% Analysis Date = 01/08/14 Pct Recovery = 44% Analysis Date = 12/30/13 Pct Recovery = 44% Analysis Date = 12/30/13 Pct Recovery = 44% Analysis Date = 12/21/13 Pct Recovery = 45% Analysis Date = 12/21/13 Pct Recovery = 45% Analysis Date = 12/11/13 Pct Recovery = 45% Analysis Date = 12/11/13 Pct Recovery = 45% Analysis Date = 12/02/13 Pct Recovery = 45% Analysis Date = 12/02/13 Pct Recovery = 45% Analysis Date = 11/22/13 Pct Recovery = 45% Analysis Date = 11/22/13 Pct Recovery = 45% Analysis Date = 11/13/13 Pct Recovery = 45% Analysis Date = 11/13/13 Pct Recovery = 45% Analysis Date = 11/04/13 Pct Recovery = 46% Analysis Date = 11/04/13 Pct Recovery = 46% Analysis Date = 10/25/13 Pct Recovery = 46% Analysis Date = 10/25/13 Pct Recovery = 46% Analysis Date = 10/16/13 Pct Recovery = 46% Analysis Date = 10/16/13 Pct Recovery = 46% Analysis Date = 10/06/13 Pct Recovery = 46% Analysis Date = 10/06/13 Pct Recovery = 46% Analysis Date = 09/27/13 Pct Recovery = 46% Analysis Date = 09/27/13 Pct Recovery = 46% Analysis Date = 09/18/13 Pct Recovery = 47% Analysis Date = 09/18/13 Pct Recovery = 47% Analysis Date = 09/08/13 Pct Recovery = 47% Analysis Date = 09/08/13 Pct Recovery = 47% Analysis Date = 08/30/13 Pct Recovery = 47% Analysis Date = 08/30/13 Pct Recovery = 47% Analysis Date = 08/20/13 Pct Recovery = 47% Analysis Date = 08/20/13 Pct Recovery = 47% Analysis Date = 08/11/13 Pct Recovery = 47% Analysis Date = 08/11/13 Pct Recovery = 47% Analysis Date = 08/02/13 Pct Recovery = 48% Analysis Date = 08/02/13 Pct Recovery = 48% Analysis Date = 07/23/13 Pct Recovery = 48% Analysis Date = 07/23/13 Pct Recovery = 48% Analysis Date = 07/14/13 Pct Recovery = 48% Analysis Date = 07/14/13 Pct Recovery = 48% Analysis Date = 07/05/13 Pct Recovery = 48% Analysis Date = 07/05/13 Pct Recovery = 48% Analysis Date = 06/25/13 Pct Recovery = 48% Analysis Date = 06/25/13 Pct Recovery = 48% Analysis Date = 06/16/13 Pct Recovery = 49% Analysis Date = 06/16/13 Pct Recovery = 49% Analysis Date = 06/06/13 Pct Recovery = 49% Analysis Date = 06/06/13 Pct Recovery = 49% Analysis Date = 05/28/13 Pct Recovery = 49% Analysis Date = 05/28/13 Pct Recovery = 49% Analysis Date = 05/19/13 Pct Recovery = 49% Analysis Date = 05/19/13 Pct Recovery = 49% Analysis Date = 05/09/13 Pct Recovery = 50% Analysis Date = 05/09/13 Pct Recovery = 50% Analysis Date = 04/30/13 Pct Recovery = 50% Analysis Date = 04/30/13 Pct Recovery = 50% Analysis Date = 04/20/13 Pct Recovery = 50% Analysis Date = 04/20/13 Pct Recovery = 50% Analysis Date = 04/11/13 Pct Recovery = 50% Analysis Date = 04/11/13 Pct Recovery = 50% Analysis Date = 04/02/13 Pct Recovery = 50% Analysis Date = 04/02/13 Pct Recovery = 50% Analysis Date = 03/23/13 Pct Recovery = 50% Analysis Date = 03/23/13 Pct Recovery = 50% Analysis Date = 03/14/13 Pct Recovery = 51% Analysis Date = 03/14/13 Pct Recovery = 51% Analysis Date = 03/04/13 Pct Recovery = 51% Analysis Date = 03/04/13 Pct Recovery = 51% Analysis Date = 02/23/13 Pct Recovery = 51% Analysis Date = 02/23/13 Pct Recovery = 51% Analysis Date = 02/14/13 Pct Recovery = 51% Analysis Date = 02/14/13 Pct Recovery = 51% Analysis Date = 02/04/13 Pct Recovery = 51% Analysis Date = 02/04/13 Pct Recovery = 51% Analysis Date = 01/26/13 Pct Recovery = 51% Analysis Date = 01/26/13 Pct Recovery = 51% Analysis Date = 01/17/13 Pct Recovery = 52% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
1-NAPHTHOL

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 7 45% 13% 41% 17%
>= Reporting Level 69 44% 18% 42% 19%
Total 76 44% 18% 42% 19%

Sample Statistics
1-NAPHTHOL

Characteristic N % % Basis
Plotted 76 100% Spiked
Estimated Values 76 100% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 76 .  
False Negatives 0 0% 0 out of 76
Not Spiked 40 .  
False Positives 2 5% 2 out of 40

OBSP Determination:
2,6-DIETHYLANILINE
METHOD: 2033 , TESTIDCODE: 82660GCM35

Laboratory ID = 20130250061 Lab Value = 0.119 Expected Conc. = 0.15 Report level label = 0.006 Pct Recovery = 79% Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl SpecificMix = A088380 Laboratory ID = 20140100085 Lab Value = 0.122 Expected Conc. = 0.1 Report level label = 0.006 Pct Recovery = 122% Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl SpecificMix = T1130514013 Laboratory ID = 20132490342 Lab Value = 0.122 Expected Conc. = 0.1 Report level label = 0.006 Pct Recovery = 122% Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl SpecificMix = T1130514013 Laboratory ID = 20140230082 Lab Value = 0.062 Expected Conc. = 0.075 Report level label = 0.006 Pct Recovery = 82% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl SpecificMix = A093651 Laboratory ID = 20132420001 Lab Value = 0.074 Expected Conc. = 0.075 Report level label = 0.006 Pct Recovery = 99% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl SpecificMix = A093651 Laboratory ID = 20130810108 Lab Value = 0.086 Expected Conc. = 0.075 Report level label = 0.006 Pct Recovery = 114% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl SpecificMix = T1120530013 Laboratory ID = 20123560092 Lab Value = 0.069 Expected Conc. = 0.075 Report level label = 0.006 Pct Recovery = 92% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = T1120530013 Laboratory ID = 20140370077 Lab Value = 0.053 Expected Conc. = 0.05 Report level label = 0.006 Pct Recovery = 105% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl SpecificMix = T1130514013 Laboratory ID = 20132690010 Lab Value = 0.070 Expected Conc. = 0.05 Report level label = 0.006 Pct Recovery = 141% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl SpecificMix = T1130514013 Laboratory ID = 20131370001 Lab Value = 0.049 Expected Conc. = 0.05 Report level label = 0.006 Pct Recovery = 97% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl SpecificMix = 1473000 Laboratory ID = 20162860079 Lab Value = 0.042 Expected Conc. = 0.04 Report level label = 0.006 Pct Recovery = 105% Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl SpecificMix = 5054800 Laboratory ID = 20161880109 Lab Value = 0.037 Expected Conc. = 0.04 Report level label = 0.006 Pct Recovery = 92% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl SpecificMix = 5054800 Laboratory ID = 20163370001 Lab Value = 0.041 Expected Conc. = 0.0375 Report level label = 0.006 Pct Recovery = 109% Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl SpecificMix = LC20138V Laboratory ID = 20152750006 Lab Value = 0.010 Expected Conc. = 0.036 Report level label = 0.006 Pct Recovery = 29% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl SpecificMix = EN150514012 Laboratory ID = 20152460215 Lab Value = 0.033 Expected Conc. = 0.036 Report level label = 0.006 Pct Recovery = 90% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl SpecificMix = EN150514012 Laboratory ID = 20171380001 Lab Value = 0.025 Expected Conc. = 0.032 Report level label = 0.006 Pct Recovery = 79% Analysis Date = 06/07/17 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 5054800 Laboratory ID = 20170960001 Lab Value = 0.027 Expected Conc. = 0.032 Report level label = 0.006 Pct Recovery = 85% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl SpecificMix = 5054800 Laboratory ID = 20161740258 Lab Value = 0.022 Expected Conc. = 0.032 Report level label = 0.006 Pct Recovery = 69% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 5054800 Laboratory ID = 20171720140 Lab Value = 0.032 Expected Conc. = 0.03 Report level label = 0.006 Pct Recovery = 106% Analysis Date = 08/31/17 SpikeMix = Supelco LC20138V: 80 µl & Phenova B20160331: 80 µl SpecificMix = LC20138V Laboratory ID = 20170740063 Lab Value = 0.031 Expected Conc. = 0.03 Report level label = 0.006 Pct Recovery = 102% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl SpecificMix = LC20138V Laboratory ID = 20161470001 Lab Value = 0.027 Expected Conc. = 0.03 Report level label = 0.006 Pct Recovery = 91% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl SpecificMix = LC20138V Laboratory ID = 20140860102 Lab Value = 0.025 Expected Conc. = 0.03 Report level label = 0.006 Pct Recovery = 84% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl SpecificMix = A093651 Laboratory ID = 20133400002 Lab Value = 0.031 Expected Conc. = 0.03 Report level label = 0.006 Pct Recovery = 103% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = A093651 Laboratory ID = 20132910008 Lab Value = 0.029 Expected Conc. = 0.03 Report level label = 0.006 Pct Recovery = 97% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = A093651 Laboratory ID = 20131920149 Lab Value = 0.029 Expected Conc. = 0.03 Report level label = 0.006 Pct Recovery = 97% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl SpecificMix = A093651 Laboratory ID = 20131230084 Lab Value = 0.032 Expected Conc. = 0.03 Report level label = 0.006 Pct Recovery = 107% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl SpecificMix = A088380 Laboratory ID = 20130650005 Lab Value = 0.026 Expected Conc. = 0.03 Report level label = 0.006 Pct Recovery = 87% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl SpecificMix = A088380 Laboratory ID = 20130390105 Lab Value = 0.032 Expected Conc. = 0.03 Report level label = 0.006 Pct Recovery = 106% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl SpecificMix = T1120530013 Laboratory ID = 20142720002 Lab Value = 0.022 Expected Conc. = 0.0241 Report level label = 0.006 Pct Recovery = 91% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl SpecificMix = LC06435 Laboratory ID = 20142530087 Lab Value = 0.021 Expected Conc. = 0.0241 Report level label = 0.006 Pct Recovery = 87% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl SpecificMix = LC06435 Laboratory ID = 20141570088 Lab Value = 0.026 Expected Conc. = 0.0241 Report level label = 0.006 Pct Recovery = 107% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl SpecificMix = LC06435 Laboratory ID = 20141220025 Lab Value = 0.021 Expected Conc. = 0.0241 Report level label = 0.006 Pct Recovery = 86% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl SpecificMix = LC06435 Laboratory ID = 20150720069 Lab Value = 0.014 Expected Conc. = 0.024 Report level label = 0.006 Pct Recovery = 59% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 03DD006 Laboratory ID = 20143110108 Lab Value = 0.014 Expected Conc. = 0.024 Report level label = 0.006 Pct Recovery = 57% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 03DD006 Laboratory ID = 20142960086 Lab Value = 0.014 Expected Conc. = 0.024 Report level label = 0.006 Pct Recovery = 60% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 03DD006 Laboratory ID = 20142270001 Lab Value = 0.013 Expected Conc. = 0.024 Report level label = 0.006 Pct Recovery = 56% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl SpecificMix = 03DD006 Laboratory ID = 20172230001 Lab Value = 0.024 Expected Conc. = 0.02 Report level label = 0.006 Pct Recovery = 121% Analysis Date = 10/19/17 SpikeMix = ChemService 6472100: 50 µl & Abs 071717Pest: 50 µl SpecificMix = 6472100 Laboratory ID = 20140730138 Lab Value = 0.019 Expected Conc. = 0.02 Report level label = 0.006 Pct Recovery = 97% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 1473000 Laboratory ID = 20133470008 Lab Value = 0.019 Expected Conc. = 0.02 Report level label = 0.006 Pct Recovery = 93% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl SpecificMix = 1473000 Laboratory ID = 20133310030 Lab Value = 0.021 Expected Conc. = 0.02 Report level label = 0.006 Pct Recovery = 107% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl SpecificMix = 1473000 Laboratory ID = 20133050050 Lab Value = 0.028 Expected Conc. = 0.02 Report level label = 0.006 Pct Recovery = 140% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl SpecificMix = T1130514013 Laboratory ID = 20132280016 Lab Value = 0.028 Expected Conc. = 0.02 Report level label = 0.006 Pct Recovery = 141% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl SpecificMix = T1130514013 Laboratory ID = 20131790009 Lab Value = 0.017 Expected Conc. = 0.02 Report level label = 0.006 Pct Recovery = 84% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl SpecificMix = 1473000 Laboratory ID = 20131650073 Lab Value = 0.020 Expected Conc. = 0.02 Report level label = 0.006 Pct Recovery = 98% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl SpecificMix = 1473000 Laboratory ID = 20160630046 Lab Value = 0.017 Expected Conc. = 0.018 Report level label = 0.006 Pct Recovery = 92% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = EN150514012 Laboratory ID = 20153440001 Lab Value = 0.016 Expected Conc. = 0.018 Report level label = 0.006 Pct Recovery = 89% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = EN150514012 Laboratory ID = 20152330039 Lab Value = 0.011 Expected Conc. = 0.018 Report level label = 0.006 Pct Recovery = 62% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl SpecificMix = 041415 Laboratory ID = 20151900132 Lab Value = 0.014 Expected Conc. = 0.018 Report level label = 0.006 Pct Recovery = 76% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl SpecificMix = 041415 Laboratory ID = 20151270112 Lab Value = 0.017 Expected Conc. = 0.018 Report level label = 0.006 Pct Recovery = 96% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl SpecificMix = 041415 Laboratory ID = 20171940002 Lab Value = 0.016 Expected Conc. = 0.016 Report level label = 0.006 Pct Recovery = 98% Analysis Date = 11/10/17 SpikeMix = ChemService 5054800: 40 µl & NSI 041816: 40 µl SpecificMix = 5054800 Laboratory ID = 20170460061 Lab Value = 0.013 Expected Conc. = 0.016 Report level label = 0.006 Pct Recovery = 79% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl SpecificMix = 5054800 Laboratory ID = 20163560019 Lab Value = 0.015 Expected Conc. = 0.016 Report level label = 0.006 Pct Recovery = 91% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl SpecificMix = 5054800 Laboratory ID = 20162150213 Lab Value = 0.013 Expected Conc. = 0.016 Report level label = 0.006 Pct Recovery = 82% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl SpecificMix = 5054800 Laboratory ID = 20171510080 Lab Value = 0.016 Expected Conc. = 0.015 Report level label = 0.006 Pct Recovery = 105% Analysis Date = 06/09/17 SpikeMix = Supelco LC20138V: 40 µl & Crescent 03FF076: 40 µl SpecificMix = LC20138V Laboratory ID = 20162520001 Lab Value = 0.016 Expected Conc. = 0.015 Report level label = 0.006 Pct Recovery = 108% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl SpecificMix = LC20138V Laboratory ID = 20162660005 Lab Value = 0.015 Expected Conc. = 0.015 Report level label = 0.006 Pct Recovery = 97% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl SpecificMix = LC20138V Laboratory ID = 20162020124 Lab Value = 0.016 Expected Conc. = 0.015 Report level label = 0.006 Pct Recovery = 104% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl SpecificMix = LC20138V Laboratory ID = 20150150115 Lab Value = 0.009 Expected Conc. = 0.0121 Report level label = 0.006 Pct Recovery = 78% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl SpecificMix = LC06435 Laboratory ID = 20143370094 Lab Value = 0.010 Expected Conc. = 0.0121 Report level label = 0.006 Pct Recovery = 80% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl SpecificMix = LC06435 Laboratory ID = 20141910243 Lab Value = 0.011 Expected Conc. = 0.0121 Report level label = 0.006 Pct Recovery = 90% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = LC06435 Laboratory ID = 20141840097 Lab Value = 0.011 Expected Conc. = 0.0121 Report level label = 0.006 Pct Recovery = 90% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl SpecificMix = LC06435 Laboratory ID = 20173120093 Lab Value = 0.013 Expected Conc. = 0.012 Report level label = 0.006 Pct Recovery = 108% Analysis Date = 03/10/18 SpikeMix = ChemService 6472100: 30 µl & ChemService 6537100: 30 µl SpecificMix = 6472100 Laboratory ID = 20142200164 Lab Value = 0.007 Expected Conc. = 0.012 Report level label = 0.006 Pct Recovery = 57% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 03DD006 Laboratory ID = 20141640076 Lab Value = 0.009 Expected Conc. = 0.012 Report level label = 0.006 Pct Recovery = 73% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = 03DD006 Laboratory ID = 20141420140 Lab Value = 0.005 Expected Conc. = 0.012 Report level label = 0.006 Pct Recovery = 44% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 03DD006 Laboratory ID = 20141080004 Lab Value = 0.007 Expected Conc. = 0.012 Report level label = 0.006 Pct Recovery = 54% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl SpecificMix = 03DD006 Laboratory ID = 20161050143 Lab Value = 0.009 Expected Conc. = 0.009 Report level label = 0.006 Pct Recovery = 101% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 041415 Laboratory ID = 20160560044 Lab Value = 0.009 Expected Conc. = 0.009 Report level label = 0.006 Pct Recovery = 94% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl SpecificMix = 041415 Laboratory ID = 20160210080 Lab Value = 0.008 Expected Conc. = 0.009 Report level label = 0.006 Pct Recovery = 89% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 041415 Laboratory ID = 20160070059 Lab Value = 0.007 Expected Conc. = 0.009 Report level label = 0.006 Pct Recovery = 82% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = EN150514012 Laboratory ID = 20153160001 Lab Value = 0.009 Expected Conc. = 0.009 Report level label = 0.006 Pct Recovery = 103% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = EN150514012 Laboratory ID = 20152950078 Lab Value = 0.006 Expected Conc. = 0.009 Report level label = 0.006 Pct Recovery = 68% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 041415 Laboratory ID = 20152040177 Lab Value = 0.008 Expected Conc. = 0.009 Report level label = 0.006 Pct Recovery = 84% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl SpecificMix = 041415 Laboratory ID = 20151760208 Lab Value = 0.006 Expected Conc. = 0.009 Report level label = 0.006 Pct Recovery = 70% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl SpecificMix = EN150514012 Laboratory ID = 20151480170 Lab Value = 0.009 Expected Conc. = 0.009 Report level label = 0.006 Pct Recovery = 97% Analysis Date = 06/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150514012 Laboratory ID = 20151210037 Lab Value = 0.009 Expected Conc. = 0.009 Report level label = 0.006 Pct Recovery = 101% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 041415 Analysis Date = 03/10/18 Pct Recovery = 108% Analysis Date = 02/28/18 Pct Recovery = 108% Analysis Date = 02/28/18 Pct Recovery = 108% Analysis Date = 02/19/18 Pct Recovery = 107% Analysis Date = 02/19/18 Pct Recovery = 107% Analysis Date = 02/09/18 Pct Recovery = 107% Analysis Date = 02/09/18 Pct Recovery = 107% Analysis Date = 01/31/18 Pct Recovery = 107% Analysis Date = 01/31/18 Pct Recovery = 107% Analysis Date = 01/22/18 Pct Recovery = 107% Analysis Date = 01/22/18 Pct Recovery = 107% Analysis Date = 01/12/18 Pct Recovery = 106% Analysis Date = 01/12/18 Pct Recovery = 106% Analysis Date = 01/03/18 Pct Recovery = 106% Analysis Date = 01/03/18 Pct Recovery = 106% Analysis Date = 12/24/17 Pct Recovery = 106% Analysis Date = 12/24/17 Pct Recovery = 106% Analysis Date = 12/15/17 Pct Recovery = 105% Analysis Date = 12/15/17 Pct Recovery = 105% Analysis Date = 12/06/17 Pct Recovery = 105% Analysis Date = 12/06/17 Pct Recovery = 105% Analysis Date = 11/26/17 Pct Recovery = 105% Analysis Date = 11/26/17 Pct Recovery = 105% Analysis Date = 11/17/17 Pct Recovery = 104% Analysis Date = 11/17/17 Pct Recovery = 104% Analysis Date = 11/07/17 Pct Recovery = 104% Analysis Date = 11/07/17 Pct Recovery = 104% Analysis Date = 10/29/17 Pct Recovery = 104% Analysis Date = 10/29/17 Pct Recovery = 104% Analysis Date = 10/20/17 Pct Recovery = 103% Analysis Date = 10/20/17 Pct Recovery = 103% Analysis Date = 10/10/17 Pct Recovery = 103% Analysis Date = 10/10/17 Pct Recovery = 103% Analysis Date = 10/01/17 Pct Recovery = 103% Analysis Date = 10/01/17 Pct Recovery = 103% Analysis Date = 09/21/17 Pct Recovery = 103% Analysis Date = 09/21/17 Pct Recovery = 103% Analysis Date = 09/12/17 Pct Recovery = 102% Analysis Date = 09/12/17 Pct Recovery = 102% Analysis Date = 09/03/17 Pct Recovery = 102% Analysis Date = 09/03/17 Pct Recovery = 102% Analysis Date = 08/24/17 Pct Recovery = 102% Analysis Date = 08/24/17 Pct Recovery = 102% Analysis Date = 08/15/17 Pct Recovery = 101% Analysis Date = 08/15/17 Pct Recovery = 101% Analysis Date = 08/05/17 Pct Recovery = 101% Analysis Date = 08/05/17 Pct Recovery = 101% Analysis Date = 07/27/17 Pct Recovery = 101% Analysis Date = 07/27/17 Pct Recovery = 101% Analysis Date = 07/18/17 Pct Recovery = 100% Analysis Date = 07/18/17 Pct Recovery = 100% Analysis Date = 07/08/17 Pct Recovery = 100% Analysis Date = 07/08/17 Pct Recovery = 100% Analysis Date = 06/29/17 Pct Recovery = 100% Analysis Date = 06/29/17 Pct Recovery = 100% Analysis Date = 06/19/17 Pct Recovery = 100% Analysis Date = 06/19/17 Pct Recovery = 100% Analysis Date = 06/10/17 Pct Recovery = 99% Analysis Date = 06/10/17 Pct Recovery = 99% Analysis Date = 06/01/17 Pct Recovery = 99% Analysis Date = 06/01/17 Pct Recovery = 99% Analysis Date = 05/22/17 Pct Recovery = 99% Analysis Date = 05/22/17 Pct Recovery = 99% Analysis Date = 05/13/17 Pct Recovery = 98% Analysis Date = 05/13/17 Pct Recovery = 98% Analysis Date = 05/03/17 Pct Recovery = 98% Analysis Date = 05/03/17 Pct Recovery = 98% Analysis Date = 04/24/17 Pct Recovery = 98% Analysis Date = 04/24/17 Pct Recovery = 98% Analysis Date = 04/15/17 Pct Recovery = 97% Analysis Date = 04/15/17 Pct Recovery = 97% Analysis Date = 04/05/17 Pct Recovery = 97% Analysis Date = 04/05/17 Pct Recovery = 97% Analysis Date = 03/27/17 Pct Recovery = 97% Analysis Date = 03/27/17 Pct Recovery = 97% Analysis Date = 03/17/17 Pct Recovery = 97% Analysis Date = 03/17/17 Pct Recovery = 97% Analysis Date = 03/08/17 Pct Recovery = 96% Analysis Date = 03/08/17 Pct Recovery = 96% Analysis Date = 02/27/17 Pct Recovery = 96% Analysis Date = 02/27/17 Pct Recovery = 96% Analysis Date = 02/17/17 Pct Recovery = 96% Analysis Date = 02/17/17 Pct Recovery = 96% Analysis Date = 02/08/17 Pct Recovery = 95% Analysis Date = 02/08/17 Pct Recovery = 95% Analysis Date = 01/29/17 Pct Recovery = 95% Analysis Date = 01/29/17 Pct Recovery = 95% Analysis Date = 01/20/17 Pct Recovery = 95% Analysis Date = 01/20/17 Pct Recovery = 95% Analysis Date = 01/11/17 Pct Recovery = 94% Analysis Date = 01/11/17 Pct Recovery = 94% Analysis Date = 01/01/17 Pct Recovery = 94% Analysis Date = 01/01/17 Pct Recovery = 94% Analysis Date = 12/23/16 Pct Recovery = 94% Analysis Date = 12/23/16 Pct Recovery = 94% Analysis Date = 12/13/16 Pct Recovery = 94% Analysis Date = 12/13/16 Pct Recovery = 94% Analysis Date = 12/04/16 Pct Recovery = 93% Analysis Date = 12/04/16 Pct Recovery = 93% Analysis Date = 11/25/16 Pct Recovery = 93% Analysis Date = 11/25/16 Pct Recovery = 93% Analysis Date = 11/15/16 Pct Recovery = 93% Analysis Date = 11/15/16 Pct Recovery = 93% Analysis Date = 11/06/16 Pct Recovery = 92% Analysis Date = 11/06/16 Pct Recovery = 92% Analysis Date = 10/27/16 Pct Recovery = 92% Analysis Date = 10/27/16 Pct Recovery = 92% Analysis Date = 10/18/16 Pct Recovery = 92% Analysis Date = 10/18/16 Pct Recovery = 92% Analysis Date = 10/09/16 Pct Recovery = 92% Analysis Date = 10/09/16 Pct Recovery = 92% Analysis Date = 09/29/16 Pct Recovery = 91% Analysis Date = 09/29/16 Pct Recovery = 91% Analysis Date = 09/20/16 Pct Recovery = 91% Analysis Date = 09/20/16 Pct Recovery = 91% Analysis Date = 09/10/16 Pct Recovery = 91% Analysis Date = 09/10/16 Pct Recovery = 91% Analysis Date = 09/01/16 Pct Recovery = 90% Analysis Date = 09/01/16 Pct Recovery = 90% Analysis Date = 08/23/16 Pct Recovery = 90% Analysis Date = 08/23/16 Pct Recovery = 90% Analysis Date = 08/13/16 Pct Recovery = 90% Analysis Date = 08/13/16 Pct Recovery = 90% Analysis Date = 08/04/16 Pct Recovery = 90% Analysis Date = 08/04/16 Pct Recovery = 90% Analysis Date = 07/25/16 Pct Recovery = 89% Analysis Date = 07/25/16 Pct Recovery = 89% Analysis Date = 07/16/16 Pct Recovery = 89% Analysis Date = 07/16/16 Pct Recovery = 89% Analysis Date = 07/07/16 Pct Recovery = 89% Analysis Date = 07/07/16 Pct Recovery = 89% Analysis Date = 06/27/16 Pct Recovery = 88% Analysis Date = 06/27/16 Pct Recovery = 88% Analysis Date = 06/18/16 Pct Recovery = 88% Analysis Date = 06/18/16 Pct Recovery = 88% Analysis Date = 06/08/16 Pct Recovery = 88% Analysis Date = 06/08/16 Pct Recovery = 88% Analysis Date = 05/30/16 Pct Recovery = 88% Analysis Date = 05/30/16 Pct Recovery = 88% Analysis Date = 05/21/16 Pct Recovery = 87% Analysis Date = 05/21/16 Pct Recovery = 87% Analysis Date = 05/11/16 Pct Recovery = 87% Analysis Date = 05/11/16 Pct Recovery = 87% Analysis Date = 05/02/16 Pct Recovery = 87% Analysis Date = 05/02/16 Pct Recovery = 87% Analysis Date = 04/22/16 Pct Recovery = 87% Analysis Date = 04/22/16 Pct Recovery = 87% Analysis Date = 04/13/16 Pct Recovery = 86% Analysis Date = 04/13/16 Pct Recovery = 86% Analysis Date = 04/04/16 Pct Recovery = 86% Analysis Date = 04/04/16 Pct Recovery = 86% Analysis Date = 03/25/16 Pct Recovery = 86% Analysis Date = 03/25/16 Pct Recovery = 86% Analysis Date = 03/16/16 Pct Recovery = 86% Analysis Date = 03/16/16 Pct Recovery = 86% Analysis Date = 03/06/16 Pct Recovery = 85% Analysis Date = 03/06/16 Pct Recovery = 85% Analysis Date = 02/26/16 Pct Recovery = 85% Analysis Date = 02/26/16 Pct Recovery = 85% Analysis Date = 02/17/16 Pct Recovery = 85% Analysis Date = 02/17/16 Pct Recovery = 85% Analysis Date = 02/07/16 Pct Recovery = 85% Analysis Date = 02/07/16 Pct Recovery = 85% Analysis Date = 01/29/16 Pct Recovery = 84% Analysis Date = 01/29/16 Pct Recovery = 84% Analysis Date = 01/19/16 Pct Recovery = 84% Analysis Date = 01/19/16 Pct Recovery = 84% Analysis Date = 01/10/16 Pct Recovery = 84% Analysis Date = 01/10/16 Pct Recovery = 84% Analysis Date = 01/01/16 Pct Recovery = 84% Analysis Date = 01/01/16 Pct Recovery = 84% Analysis Date = 12/22/15 Pct Recovery = 83% Analysis Date = 12/22/15 Pct Recovery = 83% Analysis Date = 12/13/15 Pct Recovery = 83% Analysis Date = 12/13/15 Pct Recovery = 83% Analysis Date = 12/03/15 Pct Recovery = 83% Analysis Date = 12/03/15 Pct Recovery = 83% Analysis Date = 11/24/15 Pct Recovery = 83% Analysis Date = 11/24/15 Pct Recovery = 83% Analysis Date = 11/15/15 Pct Recovery = 82% Analysis Date = 11/15/15 Pct Recovery = 82% Analysis Date = 11/05/15 Pct Recovery = 82% Analysis Date = 11/05/15 Pct Recovery = 82% Analysis Date = 10/27/15 Pct Recovery = 82% Analysis Date = 10/27/15 Pct Recovery = 82% Analysis Date = 10/17/15 Pct Recovery = 82% Analysis Date = 10/17/15 Pct Recovery = 82% Analysis Date = 10/08/15 Pct Recovery = 82% Analysis Date = 10/08/15 Pct Recovery = 82% Analysis Date = 09/29/15 Pct Recovery = 81% Analysis Date = 09/29/15 Pct Recovery = 81% Analysis Date = 09/19/15 Pct Recovery = 81% Analysis Date = 09/19/15 Pct Recovery = 81% Analysis Date = 09/10/15 Pct Recovery = 81% Analysis Date = 09/10/15 Pct Recovery = 81% Analysis Date = 08/31/15 Pct Recovery = 81% Analysis Date = 08/31/15 Pct Recovery = 81% Analysis Date = 08/22/15 Pct Recovery = 80% Analysis Date = 08/22/15 Pct Recovery = 80% Analysis Date = 08/13/15 Pct Recovery = 80% Analysis Date = 08/13/15 Pct Recovery = 80% Analysis Date = 08/03/15 Pct Recovery = 80% Analysis Date = 08/03/15 Pct Recovery = 80% Analysis Date = 07/25/15 Pct Recovery = 80% Analysis Date = 07/25/15 Pct Recovery = 80% Analysis Date = 07/15/15 Pct Recovery = 80% Analysis Date = 07/15/15 Pct Recovery = 80% Analysis Date = 07/06/15 Pct Recovery = 80% Analysis Date = 07/06/15 Pct Recovery = 80% Analysis Date = 06/27/15 Pct Recovery = 79% Analysis Date = 06/27/15 Pct Recovery = 79% Analysis Date = 06/17/15 Pct Recovery = 79% Analysis Date = 06/17/15 Pct Recovery = 79% Analysis Date = 06/08/15 Pct Recovery = 79% Analysis Date = 06/08/15 Pct Recovery = 79% Analysis Date = 05/29/15 Pct Recovery = 79% Analysis Date = 05/29/15 Pct Recovery = 79% Analysis Date = 05/20/15 Pct Recovery = 79% Analysis Date = 05/20/15 Pct Recovery = 79% Analysis Date = 05/11/15 Pct Recovery = 79% Analysis Date = 05/11/15 Pct Recovery = 79% Analysis Date = 05/01/15 Pct Recovery = 79% Analysis Date = 05/01/15 Pct Recovery = 79% Analysis Date = 04/22/15 Pct Recovery = 79% Analysis Date = 04/22/15 Pct Recovery = 79% Analysis Date = 04/12/15 Pct Recovery = 79% Analysis Date = 04/12/15 Pct Recovery = 79% Analysis Date = 04/03/15 Pct Recovery = 79% Analysis Date = 04/03/15 Pct Recovery = 79% Analysis Date = 03/25/15 Pct Recovery = 79% Analysis Date = 03/25/15 Pct Recovery = 79% Analysis Date = 03/15/15 Pct Recovery = 79% Analysis Date = 03/15/15 Pct Recovery = 79% Analysis Date = 03/06/15 Pct Recovery = 79% Analysis Date = 03/06/15 Pct Recovery = 79% Analysis Date = 02/24/15 Pct Recovery = 79% Analysis Date = 02/24/15 Pct Recovery = 79% Analysis Date = 02/15/15 Pct Recovery = 79% Analysis Date = 02/15/15 Pct Recovery = 79% Analysis Date = 02/06/15 Pct Recovery = 79% Analysis Date = 02/06/15 Pct Recovery = 79% Analysis Date = 01/27/15 Pct Recovery = 79% Analysis Date = 01/27/15 Pct Recovery = 79% Analysis Date = 01/18/15 Pct Recovery = 79% Analysis Date = 01/18/15 Pct Recovery = 79% Analysis Date = 01/08/15 Pct Recovery = 79% Analysis Date = 01/08/15 Pct Recovery = 79% Analysis Date = 12/30/14 Pct Recovery = 79% Analysis Date = 12/30/14 Pct Recovery = 79% Analysis Date = 12/21/14 Pct Recovery = 79% Analysis Date = 12/21/14 Pct Recovery = 79% Analysis Date = 12/11/14 Pct Recovery = 79% Analysis Date = 12/11/14 Pct Recovery = 79% Analysis Date = 12/02/14 Pct Recovery = 79% Analysis Date = 12/02/14 Pct Recovery = 79% Analysis Date = 11/22/14 Pct Recovery = 80% Analysis Date = 11/22/14 Pct Recovery = 80% Analysis Date = 11/13/14 Pct Recovery = 80% Analysis Date = 11/13/14 Pct Recovery = 80% Analysis Date = 11/04/14 Pct Recovery = 80% Analysis Date = 11/04/14 Pct Recovery = 80% Analysis Date = 10/25/14 Pct Recovery = 81% Analysis Date = 10/25/14 Pct Recovery = 81% Analysis Date = 10/16/14 Pct Recovery = 81% Analysis Date = 10/16/14 Pct Recovery = 81% Analysis Date = 10/06/14 Pct Recovery = 81% Analysis Date = 10/06/14 Pct Recovery = 81% Analysis Date = 09/27/14 Pct Recovery = 82% Analysis Date = 09/27/14 Pct Recovery = 82% Analysis Date = 09/18/14 Pct Recovery = 82% Analysis Date = 09/18/14 Pct Recovery = 82% Analysis Date = 09/08/14 Pct Recovery = 82% Analysis Date = 09/08/14 Pct Recovery = 82% Analysis Date = 08/30/14 Pct Recovery = 83% Analysis Date = 08/30/14 Pct Recovery = 83% Analysis Date = 08/20/14 Pct Recovery = 83% Analysis Date = 08/20/14 Pct Recovery = 83% Analysis Date = 08/11/14 Pct Recovery = 83% Analysis Date = 08/11/14 Pct Recovery = 83% Analysis Date = 08/02/14 Pct Recovery = 84% Analysis Date = 08/02/14 Pct Recovery = 84% Analysis Date = 07/23/14 Pct Recovery = 84% Analysis Date = 07/23/14 Pct Recovery = 84% Analysis Date = 07/14/14 Pct Recovery = 85% Analysis Date = 07/14/14 Pct Recovery = 85% Analysis Date = 07/04/14 Pct Recovery = 85% Analysis Date = 07/04/14 Pct Recovery = 85% Analysis Date = 06/25/14 Pct Recovery = 85% Analysis Date = 06/25/14 Pct Recovery = 85% Analysis Date = 06/16/14 Pct Recovery = 86% Analysis Date = 06/16/14 Pct Recovery = 86% Analysis Date = 06/06/14 Pct Recovery = 86% Analysis Date = 06/06/14 Pct Recovery = 86% Analysis Date = 05/28/14 Pct Recovery = 87% Analysis Date = 05/28/14 Pct Recovery = 87% Analysis Date = 05/18/14 Pct Recovery = 88% Analysis Date = 05/18/14 Pct Recovery = 88% Analysis Date = 05/09/14 Pct Recovery = 88% Analysis Date = 05/09/14 Pct Recovery = 88% Analysis Date = 04/30/14 Pct Recovery = 89% Analysis Date = 04/30/14 Pct Recovery = 89% Analysis Date = 04/20/14 Pct Recovery = 89% Analysis Date = 04/20/14 Pct Recovery = 89% Analysis Date = 04/11/14 Pct Recovery = 90% Analysis Date = 04/11/14 Pct Recovery = 90% Analysis Date = 04/01/14 Pct Recovery = 90% Analysis Date = 04/01/14 Pct Recovery = 90% Analysis Date = 03/23/14 Pct Recovery = 91% Analysis Date = 03/23/14 Pct Recovery = 91% Analysis Date = 03/14/14 Pct Recovery = 91% Analysis Date = 03/14/14 Pct Recovery = 91% Analysis Date = 03/04/14 Pct Recovery = 92% Analysis Date = 03/04/14 Pct Recovery = 92% Analysis Date = 02/23/14 Pct Recovery = 92% Analysis Date = 02/23/14 Pct Recovery = 92% Analysis Date = 02/13/14 Pct Recovery = 93% Analysis Date = 02/13/14 Pct Recovery = 93% Analysis Date = 02/04/14 Pct Recovery = 93% Analysis Date = 02/04/14 Pct Recovery = 93% Analysis Date = 01/26/14 Pct Recovery = 94% Analysis Date = 01/26/14 Pct Recovery = 94% Analysis Date = 01/16/14 Pct Recovery = 94% Analysis Date = 01/16/14 Pct Recovery = 94% Analysis Date = 01/07/14 Pct Recovery = 95% Analysis Date = 01/07/14 Pct Recovery = 95% Analysis Date = 12/28/13 Pct Recovery = 95% Analysis Date = 12/28/13 Pct Recovery = 95% Analysis Date = 12/19/13 Pct Recovery = 96% Analysis Date = 12/19/13 Pct Recovery = 96% Analysis Date = 12/10/13 Pct Recovery = 96% Analysis Date = 12/10/13 Pct Recovery = 96% Analysis Date = 11/30/13 Pct Recovery = 97% Analysis Date = 11/30/13 Pct Recovery = 97% Analysis Date = 11/21/13 Pct Recovery = 97% Analysis Date = 11/21/13 Pct Recovery = 97% Analysis Date = 11/11/13 Pct Recovery = 97% Analysis Date = 11/11/13 Pct Recovery = 97% Analysis Date = 11/02/13 Pct Recovery = 98% Analysis Date = 11/02/13 Pct Recovery = 98% Analysis Date = 10/24/13 Pct Recovery = 98% Analysis Date = 10/24/13 Pct Recovery = 98% Analysis Date = 10/14/13 Pct Recovery = 99% Analysis Date = 10/14/13 Pct Recovery = 99% Analysis Date = 10/05/13 Pct Recovery = 99% Analysis Date = 10/05/13 Pct Recovery = 99% Analysis Date = 09/25/13 Pct Recovery = 100% Analysis Date = 09/25/13 Pct Recovery = 100% Analysis Date = 09/16/13 Pct Recovery = 100% Analysis Date = 09/16/13 Pct Recovery = 100% Analysis Date = 09/07/13 Pct Recovery = 100% Analysis Date = 09/07/13 Pct Recovery = 100% Analysis Date = 08/28/13 Pct Recovery = 101% Analysis Date = 08/28/13 Pct Recovery = 101% Analysis Date = 08/19/13 Pct Recovery = 101% Analysis Date = 08/19/13 Pct Recovery = 101% Analysis Date = 08/09/13 Pct Recovery = 102% Analysis Date = 08/09/13 Pct Recovery = 102% Analysis Date = 07/31/13 Pct Recovery = 102% Analysis Date = 07/31/13 Pct Recovery = 102% Analysis Date = 07/22/13 Pct Recovery = 102% Analysis Date = 07/22/13 Pct Recovery = 102% Analysis Date = 07/12/13 Pct Recovery = 103% Analysis Date = 07/12/13 Pct Recovery = 103% Analysis Date = 07/03/13 Pct Recovery = 103% Analysis Date = 07/03/13 Pct Recovery = 103% Analysis Date = 06/23/13 Pct Recovery = 104% Analysis Date = 06/23/13 Pct Recovery = 104% Analysis Date = 06/14/13 Pct Recovery = 104% Analysis Date = 06/14/13 Pct Recovery = 104% Analysis Date = 06/05/13 Pct Recovery = 104% Analysis Date = 06/05/13 Pct Recovery = 104% Analysis Date = 05/26/13 Pct Recovery = 105% Analysis Date = 05/26/13 Pct Recovery = 105% Analysis Date = 05/17/13 Pct Recovery = 105% Analysis Date = 05/17/13 Pct Recovery = 105% Analysis Date = 05/07/13 Pct Recovery = 106% Analysis Date = 05/07/13 Pct Recovery = 106% Analysis Date = 04/28/13 Pct Recovery = 106% Analysis Date = 04/28/13 Pct Recovery = 106% Analysis Date = 04/19/13 Pct Recovery = 106% Analysis Date = 04/19/13 Pct Recovery = 106% Analysis Date = 04/09/13 Pct Recovery = 107% Analysis Date = 04/09/13 Pct Recovery = 107% Analysis Date = 03/31/13 Pct Recovery = 107% Analysis Date = 03/31/13 Pct Recovery = 107% Analysis Date = 03/21/13 Pct Recovery = 107% Analysis Date = 03/21/13 Pct Recovery = 107% Analysis Date = 03/12/13 Pct Recovery = 108% Analysis Date = 03/12/13 Pct Recovery = 108% Analysis Date = 03/03/13 Pct Recovery = 108% Analysis Date = 03/03/13 Pct Recovery = 108% Analysis Date = 02/21/13 Pct Recovery = 108% Analysis Date = 02/21/13 Pct Recovery = 108% Analysis Date = 02/12/13 Pct Recovery = 109% Analysis Date = 02/12/13 Pct Recovery = 109% Analysis Date = 02/02/13 Pct Recovery = 109% Analysis Date = 02/02/13 Pct Recovery = 109% Analysis Date = 01/24/13 Pct Recovery = 109% Analysis Date = 01/24/13 Pct Recovery = 109% Analysis Date = 01/15/13 Pct Recovery = 110% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
2,6-DIETHYLANILINE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 76 91% 21% 92% 17%
Total 76 91% 21% 92% 17%

Sample Statistics
2,6-DIETHYLANILINE

Characteristic N % % Basis
Plotted 76 100% Spiked
Estimated Values 1 1% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 76 .  
False Negatives 0 0% 0 out of 76
Not Spiked 40 .  
False Positives 0 0% 0 out of 40

OBSP Determination:
2-CHLORO-2,6-DIETHYLACETANILIDE
METHOD: 2033 , TESTIDCODE: 61618GCM39

Laboratory ID = 20132140002 Lab Value = 0.085 Expected Conc. = 0.075 Report level label = 0.01 Pct Recovery = 113% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl SpecificMix = LB99392 Laboratory ID = 20131370001 Lab Value = 0.092 Expected Conc. = 0.075 Report level label = 0.01 Pct Recovery = 122% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl SpecificMix = LB99392 Laboratory ID = 20130810108 Lab Value = 0.068 Expected Conc. = 0.075 Report level label = 0.01 Pct Recovery = 90% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl SpecificMix = LB92783 Laboratory ID = 20130100066 Lab Value = 0.077 Expected Conc. = 0.075 Report level label = 0.01 Pct Recovery = 102% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl SpecificMix = LB92783 Laboratory ID = 20172510330 Lab Value = 0.065 Expected Conc. = 0.067 Report level label = 0.01 Pct Recovery = 97% Analysis Date = 12/29/17 SpikeMix = ChemService 6537100: 100 µl & Abs 071817Pest: 100 µl SpecificMix = 071817Pest Laboratory ID = 20162860079 Lab Value = 0.070 Expected Conc. = 0.063 Report level label = 0.01 Pct Recovery = 111% Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl SpecificMix = 060916 Laboratory ID = 20163150006 Lab Value = 0.062 Expected Conc. = 0.063 Report level label = 0.01 Pct Recovery = 98% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl SpecificMix = 060916 Laboratory ID = 20152610011 Lab Value = 0.038 Expected Conc. = 0.0599 Report level label = 0.01 Pct Recovery = 63% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl SpecificMix = 0406-15-01 Laboratory ID = 20152460215 Lab Value = 0.063 Expected Conc. = 0.0599 Report level label = 0.01 Pct Recovery = 104% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl SpecificMix = 0406-15-01 Laboratory ID = 20171660002 Lab Value = 0.054 Expected Conc. = 0.0504 Report level label = 0.01 Pct Recovery = 107% Analysis Date = 08/23/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = 060916 Laboratory ID = 20170190026 Lab Value = 0.049 Expected Conc. = 0.0504 Report level label = 0.01 Pct Recovery = 97% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = 060916 Laboratory ID = 20143240095 Lab Value = 0.047 Expected Conc. = 0.0402 Report level label = 0.01 Pct Recovery = 117% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl SpecificMix = 032714 Laboratory ID = 20142270001 Lab Value = 0.034 Expected Conc. = 0.0402 Report level label = 0.01 Pct Recovery = 84% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl SpecificMix = 032714 Laboratory ID = 20141220025 Lab Value = 0.047 Expected Conc. = 0.0402 Report level label = 0.01 Pct Recovery = 116% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl SpecificMix = 032714 Laboratory ID = 20150430092 Lab Value = 0.028 Expected Conc. = 0.0401 Report level label = 0.01 Pct Recovery = 70% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl SpecificMix = E1140407002 Laboratory ID = 20143110108 Lab Value = 0.033 Expected Conc. = 0.0401 Report level label = 0.01 Pct Recovery = 83% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl SpecificMix = E1140407002 Laboratory ID = 20142720002 Lab Value = 0.034 Expected Conc. = 0.0401 Report level label = 0.01 Pct Recovery = 85% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl SpecificMix = E1140407002 Laboratory ID = 20141770149 Lab Value = 0.036 Expected Conc. = 0.0401 Report level label = 0.01 Pct Recovery = 90% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl SpecificMix = E1140407002 Laboratory ID = 20173480003 Lab Value = 0.035 Expected Conc. = 0.035 Report level label = 0.01 Pct Recovery = 100% Analysis Date = 04/05/18 SpikeMix = Abs 071717Pest: 50 µl & ChemService 6567600: 50 µl SpecificMix = 6567600 Laboratory ID = 20172560101 Lab Value = 0.026 Expected Conc. = 0.035 Report level label = 0.01 Pct Recovery = 75% Analysis Date = 12/22/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6567600: 50 µl SpecificMix = 6567600 Laboratory ID = 20181430122 Lab Value = 0.045 Expected Conc. = 0.0335 Report level label = 0.01 Pct Recovery = 133% Analysis Date = 06/20/18 SpikeMix = Abs 071817Pest: 50 µl & Spex Organics EN170808006: 50 µl SpecificMix = 071817Pest Laboratory ID = 20140510043 Lab Value = 0.031 Expected Conc. = 0.03 Report level label = 0.01 Pct Recovery = 102% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl SpecificMix = LB99392 Laboratory ID = 20133470008 Lab Value = 0.030 Expected Conc. = 0.03 Report level label = 0.01 Pct Recovery = 100% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl SpecificMix = LB99392 Laboratory ID = 20133190012 Lab Value = 0.036 Expected Conc. = 0.03 Report level label = 0.01 Pct Recovery = 119% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = LB99392 Laboratory ID = 20133050050 Lab Value = 0.038 Expected Conc. = 0.03 Report level label = 0.01 Pct Recovery = 127% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl SpecificMix = LB99392 Laboratory ID = 20130390105 Lab Value = 0.023 Expected Conc. = 0.03 Report level label = 0.01 Pct Recovery = 77% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl SpecificMix = LB92783 Laboratory ID = 20160770090 Lab Value = 0.025 Expected Conc. = 0.03 Report level label = 0.01 Pct Recovery = 84% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20160630046 Lab Value = 0.024 Expected Conc. = 0.03 Report level label = 0.01 Pct Recovery = 80% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20153510109 Lab Value = 0.022 Expected Conc. = 0.03 Report level label = 0.01 Pct Recovery = 73% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20153440001 Lab Value = 0.023 Expected Conc. = 0.03 Report level label = 0.01 Pct Recovery = 78% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20161260151 Lab Value = 0.026 Expected Conc. = 0.028 Report level label = 0.01 Pct Recovery = 91% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = 3851600 Laboratory ID = 20151550293 Lab Value = 0.035 Expected Conc. = 0.028 Report level label = 0.01 Pct Recovery = 126% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl SpecificMix = 3851600 Laboratory ID = 20151270112 Lab Value = 0.032 Expected Conc. = 0.028 Report level label = 0.01 Pct Recovery = 115% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl SpecificMix = 3851600 Laboratory ID = 20171160110 Lab Value = 0.024 Expected Conc. = 0.0252 Report level label = 0.01 Pct Recovery = 93% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = 060916 Laboratory ID = 20162520001 Lab Value = 0.033 Expected Conc. = 0.0252 Report level label = 0.01 Pct Recovery = 131% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl SpecificMix = 060916 Laboratory ID = 20163560019 Lab Value = 0.024 Expected Conc. = 0.0252 Report level label = 0.01 Pct Recovery = 95% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl SpecificMix = 060916 Laboratory ID = 20162380004 Lab Value = 0.028 Expected Conc. = 0.0252 Report level label = 0.01 Pct Recovery = 111% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = 060916 Laboratory ID = 20180730064 Lab Value = 0.030 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 149% Analysis Date = 05/16/18 SpikeMix = Abs 071717Pest: 30 µl & Abs 071817Pest: 30 µl SpecificMix = 071817Pest Laboratory ID = 20180050004 Lab Value = 0.025 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 123% Analysis Date = 04/05/18 SpikeMix = Abs 071817Pest: 30 µl & ChemService 6472100: 30 µl SpecificMix = 071817Pest Laboratory ID = 20172780018 Lab Value = 0.021 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 105% Analysis Date = 02/08/18 SpikeMix = ChemService 6537100: 30 µl & Abs 071817Pest: 30 µl SpecificMix = 071817Pest Laboratory ID = 20150150115 Lab Value = 0.017 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 87% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl SpecificMix = 032714 Laboratory ID = 20142820151 Lab Value = 0.022 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 109% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl SpecificMix = 032714 Laboratory ID = 20141490205 Lab Value = 0.025 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 122% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = 032714 Laboratory ID = 20141080004 Lab Value = 0.021 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 105% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl SpecificMix = 032714 Laboratory ID = 20142470041 Lab Value = 0.022 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 112% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141910243 Lab Value = 0.016 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 81% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141640076 Lab Value = 0.019 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 95% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141360094 Lab Value = 0.018 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 88% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = E1140407002 Laboratory ID = 20152190003 Lab Value = 0.014 Expected Conc. = 0.015 Report level label = 0.01 Pct Recovery = 91% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = 0406-15-01 Laboratory ID = 20152040177 Lab Value = 0.017 Expected Conc. = 0.015 Report level label = 0.01 Pct Recovery = 113% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl SpecificMix = 0406-15-01 Laboratory ID = 20160210080 Lab Value = 0.012 Expected Conc. = 0.014 Report level label = 0.01 Pct Recovery = 86% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 3851600 Laboratory ID = 20152950078 Lab Value = 0.010 Expected Conc. = 0.014 Report level label = 0.01 Pct Recovery = 69% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 3851600 Laboratory ID = 20153030068 Lab Value = 0.014 Expected Conc. = 0.014 Report level label = 0.01 Pct Recovery = 102% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = 3851600 Laboratory ID = 20151760208 Lab Value = 0.017 Expected Conc. = 0.014 Report level label = 0.01 Pct Recovery = 121% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl SpecificMix = 3851600 Laboratory ID = 20151380009 Lab Value = 0.014 Expected Conc. = 0.014 Report level label = 0.01 Pct Recovery = 101% Analysis Date = 05/30/15 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 3851600 Analysis Date = 06/20/18 Pct Recovery = 118% Analysis Date = 06/10/18 Pct Recovery = 118% Analysis Date = 06/10/18 Pct Recovery = 118% Analysis Date = 05/31/18 Pct Recovery = 117% Analysis Date = 05/31/18 Pct Recovery = 117% Analysis Date = 05/21/18 Pct Recovery = 117% Analysis Date = 05/21/18 Pct Recovery = 117% Analysis Date = 05/11/18 Pct Recovery = 117% Analysis Date = 05/11/18 Pct Recovery = 117% Analysis Date = 05/01/18 Pct Recovery = 116% Analysis Date = 05/01/18 Pct Recovery = 116% Analysis Date = 04/21/18 Pct Recovery = 116% Analysis Date = 04/21/18 Pct Recovery = 116% Analysis Date = 04/11/18 Pct Recovery = 115% Analysis Date = 04/11/18 Pct Recovery = 115% Analysis Date = 04/01/18 Pct Recovery = 115% Analysis Date = 04/01/18 Pct Recovery = 115% Analysis Date = 03/22/18 Pct Recovery = 115% Analysis Date = 03/22/18 Pct Recovery = 115% Analysis Date = 03/13/18 Pct Recovery = 114% Analysis Date = 03/13/18 Pct Recovery = 114% Analysis Date = 03/03/18 Pct Recovery = 114% Analysis Date = 03/03/18 Pct Recovery = 114% Analysis Date = 02/21/18 Pct Recovery = 114% Analysis Date = 02/21/18 Pct Recovery = 114% Analysis Date = 02/11/18 Pct Recovery = 113% Analysis Date = 02/11/18 Pct Recovery = 113% Analysis Date = 02/01/18 Pct Recovery = 113% Analysis Date = 02/01/18 Pct Recovery = 113% Analysis Date = 01/22/18 Pct Recovery = 113% Analysis Date = 01/22/18 Pct Recovery = 113% Analysis Date = 01/12/18 Pct Recovery = 112% Analysis Date = 01/12/18 Pct Recovery = 112% Analysis Date = 01/02/18 Pct Recovery = 112% Analysis Date = 01/02/18 Pct Recovery = 112% Analysis Date = 12/23/17 Pct Recovery = 111% Analysis Date = 12/23/17 Pct Recovery = 111% Analysis Date = 12/13/17 Pct Recovery = 111% Analysis Date = 12/13/17 Pct Recovery = 111% Analysis Date = 12/04/17 Pct Recovery = 111% Analysis Date = 12/04/17 Pct Recovery = 111% Analysis Date = 11/24/17 Pct Recovery = 110% Analysis Date = 11/24/17 Pct Recovery = 110% Analysis Date = 11/14/17 Pct Recovery = 110% Analysis Date = 11/14/17 Pct Recovery = 110% Analysis Date = 11/04/17 Pct Recovery = 110% Analysis Date = 11/04/17 Pct Recovery = 110% Analysis Date = 10/25/17 Pct Recovery = 109% Analysis Date = 10/25/17 Pct Recovery = 109% Analysis Date = 10/15/17 Pct Recovery = 109% Analysis Date = 10/15/17 Pct Recovery = 109% Analysis Date = 10/05/17 Pct Recovery = 108% Analysis Date = 10/05/17 Pct Recovery = 108% Analysis Date = 09/25/17 Pct Recovery = 108% Analysis Date = 09/25/17 Pct Recovery = 108% Analysis Date = 09/15/17 Pct Recovery = 108% Analysis Date = 09/15/17 Pct Recovery = 108% Analysis Date = 09/05/17 Pct Recovery = 107% Analysis Date = 09/05/17 Pct Recovery = 107% Analysis Date = 08/27/17 Pct Recovery = 107% Analysis Date = 08/27/17 Pct Recovery = 107% Analysis Date = 08/17/17 Pct Recovery = 107% Analysis Date = 08/17/17 Pct Recovery = 107% Analysis Date = 08/07/17 Pct Recovery = 106% Analysis Date = 08/07/17 Pct Recovery = 106% Analysis Date = 07/28/17 Pct Recovery = 106% Analysis Date = 07/28/17 Pct Recovery = 106% Analysis Date = 07/18/17 Pct Recovery = 105% Analysis Date = 07/18/17 Pct Recovery = 105% Analysis Date = 07/08/17 Pct Recovery = 105% Analysis Date = 07/08/17 Pct Recovery = 105% Analysis Date = 06/28/17 Pct Recovery = 105% Analysis Date = 06/28/17 Pct Recovery = 105% Analysis Date = 06/18/17 Pct Recovery = 104% Analysis Date = 06/18/17 Pct Recovery = 104% Analysis Date = 06/08/17 Pct Recovery = 104% Analysis Date = 06/08/17 Pct Recovery = 104% Analysis Date = 05/29/17 Pct Recovery = 104% Analysis Date = 05/29/17 Pct Recovery = 104% Analysis Date = 05/20/17 Pct Recovery = 103% Analysis Date = 05/20/17 Pct Recovery = 103% Analysis Date = 05/10/17 Pct Recovery = 103% Analysis Date = 05/10/17 Pct Recovery = 103% Analysis Date = 04/30/17 Pct Recovery = 103% Analysis Date = 04/30/17 Pct Recovery = 103% Analysis Date = 04/20/17 Pct Recovery = 102% Analysis Date = 04/20/17 Pct Recovery = 102% Analysis Date = 04/10/17 Pct Recovery = 102% Analysis Date = 04/10/17 Pct Recovery = 102% Analysis Date = 03/31/17 Pct Recovery = 101% Analysis Date = 03/31/17 Pct Recovery = 101% Analysis Date = 03/21/17 Pct Recovery = 101% Analysis Date = 03/21/17 Pct Recovery = 101% Analysis Date = 03/11/17 Pct Recovery = 101% Analysis Date = 03/11/17 Pct Recovery = 101% Analysis Date = 03/01/17 Pct Recovery = 100% Analysis Date = 03/01/17 Pct Recovery = 100% Analysis Date = 02/19/17 Pct Recovery = 100% Analysis Date = 02/19/17 Pct Recovery = 100% Analysis Date = 02/10/17 Pct Recovery = 100% Analysis Date = 02/10/17 Pct Recovery = 100% Analysis Date = 01/31/17 Pct Recovery = 100% Analysis Date = 01/31/17 Pct Recovery = 100% Analysis Date = 01/21/17 Pct Recovery = 99% Analysis Date = 01/21/17 Pct Recovery = 99% Analysis Date = 01/11/17 Pct Recovery = 99% Analysis Date = 01/11/17 Pct Recovery = 99% Analysis Date = 01/01/17 Pct Recovery = 99% Analysis Date = 01/01/17 Pct Recovery = 99% Analysis Date = 12/22/16 Pct Recovery = 99% Analysis Date = 12/22/16 Pct Recovery = 99% Analysis Date = 12/12/16 Pct Recovery = 99% Analysis Date = 12/12/16 Pct Recovery = 99% Analysis Date = 12/02/16 Pct Recovery = 99% Analysis Date = 12/02/16 Pct Recovery = 99% Analysis Date = 11/22/16 Pct Recovery = 98% Analysis Date = 11/22/16 Pct Recovery = 98% Analysis Date = 11/12/16 Pct Recovery = 98% Analysis Date = 11/12/16 Pct Recovery = 98% Analysis Date = 11/03/16 Pct Recovery = 98% Analysis Date = 11/03/16 Pct Recovery = 98% Analysis Date = 10/24/16 Pct Recovery = 98% Analysis Date = 10/24/16 Pct Recovery = 98% Analysis Date = 10/14/16 Pct Recovery = 98% Analysis Date = 10/14/16 Pct Recovery = 98% Analysis Date = 10/04/16 Pct Recovery = 98% Analysis Date = 10/04/16 Pct Recovery = 98% Analysis Date = 09/24/16 Pct Recovery = 97% Analysis Date = 09/24/16 Pct Recovery = 97% Analysis Date = 09/14/16 Pct Recovery = 97% Analysis Date = 09/14/16 Pct Recovery = 97% Analysis Date = 09/04/16 Pct Recovery = 97% Analysis Date = 09/04/16 Pct Recovery = 97% Analysis Date = 08/25/16 Pct Recovery = 97% Analysis Date = 08/25/16 Pct Recovery = 97% Analysis Date = 08/15/16 Pct Recovery = 97% Analysis Date = 08/15/16 Pct Recovery = 97% Analysis Date = 08/05/16 Pct Recovery = 97% Analysis Date = 08/05/16 Pct Recovery = 97% Analysis Date = 07/27/16 Pct Recovery = 96% Analysis Date = 07/27/16 Pct Recovery = 96% Analysis Date = 07/17/16 Pct Recovery = 96% Analysis Date = 07/17/16 Pct Recovery = 96% Analysis Date = 07/07/16 Pct Recovery = 96% Analysis Date = 07/07/16 Pct Recovery = 96% Analysis Date = 06/27/16 Pct Recovery = 96% Analysis Date = 06/27/16 Pct Recovery = 96% Analysis Date = 06/17/16 Pct Recovery = 96% Analysis Date = 06/17/16 Pct Recovery = 96% Analysis Date = 06/07/16 Pct Recovery = 96% Analysis Date = 06/07/16 Pct Recovery = 96% Analysis Date = 05/28/16 Pct Recovery = 95% Analysis Date = 05/28/16 Pct Recovery = 95% Analysis Date = 05/18/16 Pct Recovery = 95% Analysis Date = 05/18/16 Pct Recovery = 95% Analysis Date = 05/08/16 Pct Recovery = 95% Analysis Date = 05/08/16 Pct Recovery = 95% Analysis Date = 04/28/16 Pct Recovery = 95% Analysis Date = 04/28/16 Pct Recovery = 95% Analysis Date = 04/19/16 Pct Recovery = 95% Analysis Date = 04/19/16 Pct Recovery = 95% Analysis Date = 04/09/16 Pct Recovery = 95% Analysis Date = 04/09/16 Pct Recovery = 95% Analysis Date = 03/30/16 Pct Recovery = 94% Analysis Date = 03/30/16 Pct Recovery = 94% Analysis Date = 03/20/16 Pct Recovery = 94% Analysis Date = 03/20/16 Pct Recovery = 94% Analysis Date = 03/10/16 Pct Recovery = 94% Analysis Date = 03/10/16 Pct Recovery = 94% Analysis Date = 02/29/16 Pct Recovery = 94% Analysis Date = 02/29/16 Pct Recovery = 94% Analysis Date = 02/19/16 Pct Recovery = 94% Analysis Date = 02/19/16 Pct Recovery = 94% Analysis Date = 02/09/16 Pct Recovery = 93% Analysis Date = 02/09/16 Pct Recovery = 93% Analysis Date = 01/30/16 Pct Recovery = 93% Analysis Date = 01/30/16 Pct Recovery = 93% Analysis Date = 01/20/16 Pct Recovery = 93% Analysis Date = 01/20/16 Pct Recovery = 93% Analysis Date = 01/11/16 Pct Recovery = 93% Analysis Date = 01/11/16 Pct Recovery = 93% Analysis Date = 01/01/16 Pct Recovery = 93% Analysis Date = 01/01/16 Pct Recovery = 93% Analysis Date = 12/22/15 Pct Recovery = 93% Analysis Date = 12/22/15 Pct Recovery = 93% Analysis Date = 12/12/15 Pct Recovery = 93% Analysis Date = 12/12/15 Pct Recovery = 93% Analysis Date = 12/02/15 Pct Recovery = 93% Analysis Date = 12/02/15 Pct Recovery = 93% Analysis Date = 11/22/15 Pct Recovery = 93% Analysis Date = 11/22/15 Pct Recovery = 93% Analysis Date = 11/12/15 Pct Recovery = 93% Analysis Date = 11/12/15 Pct Recovery = 93% Analysis Date = 11/02/15 Pct Recovery = 93% Analysis Date = 11/02/15 Pct Recovery = 93% Analysis Date = 10/23/15 Pct Recovery = 93% Analysis Date = 10/23/15 Pct Recovery = 93% Analysis Date = 10/13/15 Pct Recovery = 93% Analysis Date = 10/13/15 Pct Recovery = 93% Analysis Date = 10/04/15 Pct Recovery = 93% Analysis Date = 10/04/15 Pct Recovery = 93% Analysis Date = 09/24/15 Pct Recovery = 93% Analysis Date = 09/24/15 Pct Recovery = 93% Analysis Date = 09/14/15 Pct Recovery = 93% Analysis Date = 09/14/15 Pct Recovery = 93% Analysis Date = 09/04/15 Pct Recovery = 93% Analysis Date = 09/04/15 Pct Recovery = 93% Analysis Date = 08/25/15 Pct Recovery = 93% Analysis Date = 08/25/15 Pct Recovery = 93% Analysis Date = 08/15/15 Pct Recovery = 93% Analysis Date = 08/15/15 Pct Recovery = 93% Analysis Date = 08/05/15 Pct Recovery = 93% Analysis Date = 08/05/15 Pct Recovery = 93% Analysis Date = 07/26/15 Pct Recovery = 94% Analysis Date = 07/26/15 Pct Recovery = 94% Analysis Date = 07/16/15 Pct Recovery = 94% Analysis Date = 07/16/15 Pct Recovery = 94% Analysis Date = 07/06/15 Pct Recovery = 94% Analysis Date = 07/06/15 Pct Recovery = 94% Analysis Date = 06/27/15 Pct Recovery = 94% Analysis Date = 06/27/15 Pct Recovery = 94% Analysis Date = 06/17/15 Pct Recovery = 95% Analysis Date = 06/17/15 Pct Recovery = 95% Analysis Date = 06/07/15 Pct Recovery = 95% Analysis Date = 06/07/15 Pct Recovery = 95% Analysis Date = 05/28/15 Pct Recovery = 95% Analysis Date = 05/28/15 Pct Recovery = 95% Analysis Date = 05/18/15 Pct Recovery = 96% Analysis Date = 05/18/15 Pct Recovery = 96% Analysis Date = 05/08/15 Pct Recovery = 96% Analysis Date = 05/08/15 Pct Recovery = 96% Analysis Date = 04/28/15 Pct Recovery = 96% Analysis Date = 04/28/15 Pct Recovery = 96% Analysis Date = 04/18/15 Pct Recovery = 96% Analysis Date = 04/18/15 Pct Recovery = 96% Analysis Date = 04/08/15 Pct Recovery = 96% Analysis Date = 04/08/15 Pct Recovery = 96% Analysis Date = 03/29/15 Pct Recovery = 97% Analysis Date = 03/29/15 Pct Recovery = 97% Analysis Date = 03/20/15 Pct Recovery = 97% Analysis Date = 03/20/15 Pct Recovery = 97% Analysis Date = 03/10/15 Pct Recovery = 97% Analysis Date = 03/10/15 Pct Recovery = 97% Analysis Date = 02/28/15 Pct Recovery = 97% Analysis Date = 02/28/15 Pct Recovery = 97% Analysis Date = 02/18/15 Pct Recovery = 97% Analysis Date = 02/18/15 Pct Recovery = 97% Analysis Date = 02/08/15 Pct Recovery = 98% Analysis Date = 02/08/15 Pct Recovery = 98% Analysis Date = 01/29/15 Pct Recovery = 98% Analysis Date = 01/29/15 Pct Recovery = 98% Analysis Date = 01/19/15 Pct Recovery = 98% Analysis Date = 01/19/15 Pct Recovery = 98% Analysis Date = 01/09/15 Pct Recovery = 98% Analysis Date = 01/09/15 Pct Recovery = 98% Analysis Date = 12/30/14 Pct Recovery = 99% Analysis Date = 12/30/14 Pct Recovery = 99% Analysis Date = 12/20/14 Pct Recovery = 99% Analysis Date = 12/20/14 Pct Recovery = 99% Analysis Date = 12/11/14 Pct Recovery = 99% Analysis Date = 12/11/14 Pct Recovery = 99% Analysis Date = 12/01/14 Pct Recovery = 99% Analysis Date = 12/01/14 Pct Recovery = 99% Analysis Date = 11/21/14 Pct Recovery = 99% Analysis Date = 11/21/14 Pct Recovery = 99% Analysis Date = 11/11/14 Pct Recovery = 100% Analysis Date = 11/11/14 Pct Recovery = 100% Analysis Date = 11/01/14 Pct Recovery = 100% Analysis Date = 11/01/14 Pct Recovery = 100% Analysis Date = 10/22/14 Pct Recovery = 100% Analysis Date = 10/22/14 Pct Recovery = 100% Analysis Date = 10/12/14 Pct Recovery = 100% Analysis Date = 10/12/14 Pct Recovery = 100% Analysis Date = 10/02/14 Pct Recovery = 100% Analysis Date = 10/02/14 Pct Recovery = 100% Analysis Date = 09/22/14 Pct Recovery = 100% Analysis Date = 09/22/14 Pct Recovery = 100% Analysis Date = 09/12/14 Pct Recovery = 100% Analysis Date = 09/12/14 Pct Recovery = 100% Analysis Date = 09/03/14 Pct Recovery = 101% Analysis Date = 09/03/14 Pct Recovery = 101% Analysis Date = 08/24/14 Pct Recovery = 101% Analysis Date = 08/24/14 Pct Recovery = 101% Analysis Date = 08/14/14 Pct Recovery = 101% Analysis Date = 08/14/14 Pct Recovery = 101% Analysis Date = 08/04/14 Pct Recovery = 101% Analysis Date = 08/04/14 Pct Recovery = 101% Analysis Date = 07/25/14 Pct Recovery = 101% Analysis Date = 07/25/14 Pct Recovery = 101% Analysis Date = 07/15/14 Pct Recovery = 102% Analysis Date = 07/15/14 Pct Recovery = 102% Analysis Date = 07/05/14 Pct Recovery = 102% Analysis Date = 07/05/14 Pct Recovery = 102% Analysis Date = 06/25/14 Pct Recovery = 102% Analysis Date = 06/25/14 Pct Recovery = 102% Analysis Date = 06/15/14 Pct Recovery = 102% Analysis Date = 06/15/14 Pct Recovery = 102% Analysis Date = 06/05/14 Pct Recovery = 102% Analysis Date = 06/05/14 Pct Recovery = 102% Analysis Date = 05/27/14 Pct Recovery = 102% Analysis Date = 05/27/14 Pct Recovery = 102% Analysis Date = 05/17/14 Pct Recovery = 102% Analysis Date = 05/17/14 Pct Recovery = 102% Analysis Date = 05/07/14 Pct Recovery = 102% Analysis Date = 05/07/14 Pct Recovery = 102% Analysis Date = 04/27/14 Pct Recovery = 102% Analysis Date = 04/27/14 Pct Recovery = 102% Analysis Date = 04/17/14 Pct Recovery = 102% Analysis Date = 04/17/14 Pct Recovery = 102% Analysis Date = 04/07/14 Pct Recovery = 102% Analysis Date = 04/07/14 Pct Recovery = 102% Analysis Date = 03/28/14 Pct Recovery = 102% Analysis Date = 03/28/14 Pct Recovery = 102% Analysis Date = 03/18/14 Pct Recovery = 102% Analysis Date = 03/18/14 Pct Recovery = 102% Analysis Date = 03/08/14 Pct Recovery = 102% Analysis Date = 03/08/14 Pct Recovery = 102% Analysis Date = 02/26/14 Pct Recovery = 102% Analysis Date = 02/26/14 Pct Recovery = 102% Analysis Date = 02/17/14 Pct Recovery = 102% Analysis Date = 02/17/14 Pct Recovery = 102% Analysis Date = 02/07/14 Pct Recovery = 103% Analysis Date = 02/07/14 Pct Recovery = 103% Analysis Date = 01/28/14 Pct Recovery = 103% Analysis Date = 01/28/14 Pct Recovery = 103% Analysis Date = 01/18/14 Pct Recovery = 103% Analysis Date = 01/18/14 Pct Recovery = 103% Analysis Date = 01/08/14 Pct Recovery = 103% Analysis Date = 01/08/14 Pct Recovery = 103% Analysis Date = 12/29/13 Pct Recovery = 103% Analysis Date = 12/29/13 Pct Recovery = 103% Analysis Date = 12/19/13 Pct Recovery = 103% Analysis Date = 12/19/13 Pct Recovery = 103% Analysis Date = 12/09/13 Pct Recovery = 103% Analysis Date = 12/09/13 Pct Recovery = 103% Analysis Date = 11/29/13 Pct Recovery = 103% Analysis Date = 11/29/13 Pct Recovery = 103% Analysis Date = 11/19/13 Pct Recovery = 103% Analysis Date = 11/19/13 Pct Recovery = 103% Analysis Date = 11/10/13 Pct Recovery = 103% Analysis Date = 11/10/13 Pct Recovery = 103% Analysis Date = 10/31/13 Pct Recovery = 103% Analysis Date = 10/31/13 Pct Recovery = 103% Analysis Date = 10/21/13 Pct Recovery = 103% Analysis Date = 10/21/13 Pct Recovery = 103% Analysis Date = 10/11/13 Pct Recovery = 103% Analysis Date = 10/11/13 Pct Recovery = 103% Analysis Date = 10/01/13 Pct Recovery = 103% Analysis Date = 10/01/13 Pct Recovery = 103% Analysis Date = 09/21/13 Pct Recovery = 103% Analysis Date = 09/21/13 Pct Recovery = 103% Analysis Date = 09/11/13 Pct Recovery = 103% Analysis Date = 09/11/13 Pct Recovery = 103% Analysis Date = 09/01/13 Pct Recovery = 103% Analysis Date = 09/01/13 Pct Recovery = 103% Analysis Date = 08/22/13 Pct Recovery = 103% Analysis Date = 08/22/13 Pct Recovery = 103% Analysis Date = 08/12/13 Pct Recovery = 103% Analysis Date = 08/12/13 Pct Recovery = 103% Analysis Date = 08/03/13 Pct Recovery = 103% Analysis Date = 08/03/13 Pct Recovery = 103% Analysis Date = 07/24/13 Pct Recovery = 103% Analysis Date = 07/24/13 Pct Recovery = 103% Analysis Date = 07/14/13 Pct Recovery = 103% Analysis Date = 07/14/13 Pct Recovery = 103% Analysis Date = 07/04/13 Pct Recovery = 103% Analysis Date = 07/04/13 Pct Recovery = 103% Analysis Date = 06/24/13 Pct Recovery = 103% Analysis Date = 06/24/13 Pct Recovery = 103% Analysis Date = 06/14/13 Pct Recovery = 103% Analysis Date = 06/14/13 Pct Recovery = 103% Analysis Date = 06/04/13 Pct Recovery = 103% Analysis Date = 06/04/13 Pct Recovery = 103% Analysis Date = 05/25/13 Pct Recovery = 104% Analysis Date = 05/25/13 Pct Recovery = 104% Analysis Date = 05/15/13 Pct Recovery = 104% Analysis Date = 05/15/13 Pct Recovery = 104% Analysis Date = 05/05/13 Pct Recovery = 104% Analysis Date = 05/05/13 Pct Recovery = 104% Analysis Date = 04/26/13 Pct Recovery = 104% Analysis Date = 04/26/13 Pct Recovery = 104% Analysis Date = 04/16/13 Pct Recovery = 104% Analysis Date = 04/16/13 Pct Recovery = 104% Analysis Date = 04/06/13 Pct Recovery = 104% Analysis Date = 04/06/13 Pct Recovery = 104% Analysis Date = 03/27/13 Pct Recovery = 104% Analysis Date = 03/27/13 Pct Recovery = 104% Analysis Date = 03/17/13 Pct Recovery = 104% Analysis Date = 03/17/13 Pct Recovery = 104% Analysis Date = 03/07/13 Pct Recovery = 104% Analysis Date = 03/07/13 Pct Recovery = 104% Analysis Date = 02/25/13 Pct Recovery = 104% Analysis Date = 02/25/13 Pct Recovery = 104% Analysis Date = 02/15/13 Pct Recovery = 104% Analysis Date = 02/15/13 Pct Recovery = 104% Analysis Date = 02/05/13 Pct Recovery = 104% Analysis Date = 02/05/13 Pct Recovery = 104% Analysis Date = 01/26/13 Pct Recovery = 104% Analysis Date = 01/26/13 Pct Recovery = 104% Analysis Date = 01/17/13 Pct Recovery = 104% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
2-CHLORO-2,6-DIETHYLACETANILIDE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 55 100% 18% 100% 21%
Total 55 100% 18% 100% 21%

Sample Statistics
2-CHLORO-2,6-DIETHYLACETANILIDE

Characteristic N % % Basis
Plotted 55 98% Spiked
Estimated Values 1 2% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 1 2% Spiked
Spiked 56 .  
False Negatives 0 0% 0 out of 56
Not Spiked 78 .  
False Positives 0 0% 0 out of 78

OBSP Determination:
2-ETHYL-6-METHYLANILINE
METHOD: 2033 , TESTIDCODE: 61620GCM39

Laboratory ID = 20140100085 Lab Value = 0.139 Expected Conc. = 0.15 Report level label = 0.01 Pct Recovery = 93% Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl SpecificMix = T1130514013 Laboratory ID = 20132490342 Lab Value = 0.162 Expected Conc. = 0.15 Report level label = 0.01 Pct Recovery = 108% Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl SpecificMix = T1130514013 Laboratory ID = 20131370001 Lab Value = 0.076 Expected Conc. = 0.076 Report level label = 0.01 Pct Recovery = 100% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl SpecificMix = 1473000 Laboratory ID = 20130940097 Lab Value = 0.075 Expected Conc. = 0.0755 Report level label = 0.01 Pct Recovery = 99% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = 0507-12-04.2 Laboratory ID = 20123560092 Lab Value = 0.058 Expected Conc. = 0.0755 Report level label = 0.01 Pct Recovery = 77% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = 0507-12-04.2 Laboratory ID = 20140370077 Lab Value = 0.069 Expected Conc. = 0.075 Report level label = 0.01 Pct Recovery = 92% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl SpecificMix = T1130514013 Laboratory ID = 20132690010 Lab Value = 0.090 Expected Conc. = 0.075 Report level label = 0.01 Pct Recovery = 119% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl SpecificMix = T1130514013 Laboratory ID = 20163370001 Lab Value = 0.059 Expected Conc. = 0.0623 Report level label = 0.01 Pct Recovery = 95% Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl SpecificMix = LC20138V Laboratory ID = 20162860079 Lab Value = 0.063 Expected Conc. = 0.06 Report level label = 0.01 Pct Recovery = 105% Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl SpecificMix = 5054800 Laboratory ID = 20161880109 Lab Value = 0.051 Expected Conc. = 0.06 Report level label = 0.01 Pct Recovery = 85% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl SpecificMix = 5054800 Laboratory ID = 20152610011 Lab Value = 0.048 Expected Conc. = 0.06 Report level label = 0.01 Pct Recovery = 80% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl SpecificMix = 040615 Laboratory ID = 20171720140 Lab Value = 0.044 Expected Conc. = 0.0498 Report level label = 0.01 Pct Recovery = 89% Analysis Date = 08/31/17 SpikeMix = Supelco LC20138V: 80 µl & Phenova B20160331: 80 µl SpecificMix = LC20138V Laboratory ID = 20170740063 Lab Value = 0.040 Expected Conc. = 0.0498 Report level label = 0.01 Pct Recovery = 80% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl SpecificMix = LC20138V Laboratory ID = 20161470001 Lab Value = 0.037 Expected Conc. = 0.0498 Report level label = 0.01 Pct Recovery = 74% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl SpecificMix = LC20138V Laboratory ID = 20171380001 Lab Value = 0.037 Expected Conc. = 0.048 Report level label = 0.01 Pct Recovery = 78% Analysis Date = 06/07/17 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 5054800 Laboratory ID = 20170960001 Lab Value = 0.039 Expected Conc. = 0.048 Report level label = 0.01 Pct Recovery = 81% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl SpecificMix = 5054800 Laboratory ID = 20161740258 Lab Value = 0.035 Expected Conc. = 0.048 Report level label = 0.01 Pct Recovery = 73% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 5054800 Laboratory ID = 20150430092 Lab Value = 0.038 Expected Conc. = 0.0402 Report level label = 0.01 Pct Recovery = 94% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl SpecificMix = E1140407002 Laboratory ID = 20143240095 Lab Value = 0.034 Expected Conc. = 0.0402 Report level label = 0.01 Pct Recovery = 85% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl SpecificMix = 032714 Laboratory ID = 20143110108 Lab Value = 0.037 Expected Conc. = 0.0402 Report level label = 0.01 Pct Recovery = 92% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl SpecificMix = E1140407002 Laboratory ID = 20142720002 Lab Value = 0.036 Expected Conc. = 0.0402 Report level label = 0.01 Pct Recovery = 89% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl SpecificMix = E1140407002 Laboratory ID = 20142270001 Lab Value = 0.037 Expected Conc. = 0.0402 Report level label = 0.01 Pct Recovery = 91% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl SpecificMix = 032714 Laboratory ID = 20141770149 Lab Value = 0.037 Expected Conc. = 0.0402 Report level label = 0.01 Pct Recovery = 91% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl SpecificMix = E1140407002 Laboratory ID = 20141220025 Lab Value = 0.033 Expected Conc. = 0.0402 Report level label = 0.01 Pct Recovery = 83% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl SpecificMix = 032714 Laboratory ID = 20172230001 Lab Value = 0.037 Expected Conc. = 0.035 Report level label = 0.01 Pct Recovery = 105% Analysis Date = 10/19/17 SpikeMix = ChemService 6472100: 50 µl & Abs 071717Pest: 50 µl SpecificMix = 6472100 Laboratory ID = 20172560101 Lab Value = 0.029 Expected Conc. = 0.0332 Report level label = 0.01 Pct Recovery = 86% Analysis Date = 12/22/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6567600: 50 µl SpecificMix = EN170808006 Laboratory ID = 20172370001 Lab Value = 0.031 Expected Conc. = 0.0332 Report level label = 0.01 Pct Recovery = 94% Analysis Date = 11/18/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6537100: 50 µl SpecificMix = EN170808006 Laboratory ID = 20140730138 Lab Value = 0.025 Expected Conc. = 0.0304 Report level label = 0.01 Pct Recovery = 81% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 1473000 Laboratory ID = 20133470008 Lab Value = 0.029 Expected Conc. = 0.0304 Report level label = 0.01 Pct Recovery = 95% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl SpecificMix = 1473000 Laboratory ID = 20133310030 Lab Value = 0.036 Expected Conc. = 0.0304 Report level label = 0.01 Pct Recovery = 119% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl SpecificMix = 1473000 Laboratory ID = 20131790009 Lab Value = 0.022 Expected Conc. = 0.0304 Report level label = 0.01 Pct Recovery = 72% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl SpecificMix = 1473000 Laboratory ID = 20131650073 Lab Value = 0.025 Expected Conc. = 0.0304 Report level label = 0.01 Pct Recovery = 82% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl SpecificMix = 1473000 Laboratory ID = 20130510051 Lab Value = 0.024 Expected Conc. = 0.0302 Report level label = 0.01 Pct Recovery = 81% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl SpecificMix = 0507-12-04.2 Laboratory ID = 20161260151 Lab Value = 0.024 Expected Conc. = 0.03 Report level label = 0.01 Pct Recovery = 80% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = EN150513008 Laboratory ID = 20160770090 Lab Value = 0.027 Expected Conc. = 0.03 Report level label = 0.01 Pct Recovery = 90% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = EN150513008 Laboratory ID = 20153510109 Lab Value = 0.023 Expected Conc. = 0.03 Report level label = 0.01 Pct Recovery = 78% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = EN150513008 Laboratory ID = 20152330039 Lab Value = 0.017 Expected Conc. = 0.03 Report level label = 0.01 Pct Recovery = 55% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl SpecificMix = EN150513008 Laboratory ID = 20151900132 Lab Value = 0.021 Expected Conc. = 0.03 Report level label = 0.01 Pct Recovery = 71% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl SpecificMix = 040615 Laboratory ID = 20151550293 Lab Value = 0.025 Expected Conc. = 0.03 Report level label = 0.01 Pct Recovery = 82% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl SpecificMix = 040615 Laboratory ID = 20133050050 Lab Value = 0.037 Expected Conc. = 0.03 Report level label = 0.01 Pct Recovery = 124% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl SpecificMix = T1130514013 Laboratory ID = 20132280016 Lab Value = 0.035 Expected Conc. = 0.03 Report level label = 0.01 Pct Recovery = 116% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl SpecificMix = T1130514013 Laboratory ID = 20171510080 Lab Value = 0.023 Expected Conc. = 0.0249 Report level label = 0.01 Pct Recovery = 92% Analysis Date = 06/09/17 SpikeMix = Supelco LC20138V: 40 µl & Crescent 03FF076: 40 µl SpecificMix = LC20138V Laboratory ID = 20162520001 Lab Value = 0.021 Expected Conc. = 0.0249 Report level label = 0.01 Pct Recovery = 86% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl SpecificMix = LC20138V Laboratory ID = 20162660005 Lab Value = 0.021 Expected Conc. = 0.0249 Report level label = 0.01 Pct Recovery = 84% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl SpecificMix = LC20138V Laboratory ID = 20162020124 Lab Value = 0.022 Expected Conc. = 0.0249 Report level label = 0.01 Pct Recovery = 89% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl SpecificMix = LC20138V Laboratory ID = 20171940002 Lab Value = 0.022 Expected Conc. = 0.024 Report level label = 0.01 Pct Recovery = 92% Analysis Date = 11/10/17 SpikeMix = ChemService 5054800: 40 µl & NSI 041816: 40 µl SpecificMix = 5054800 Laboratory ID = 20170460061 Lab Value = 0.018 Expected Conc. = 0.024 Report level label = 0.01 Pct Recovery = 75% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl SpecificMix = 5054800 Laboratory ID = 20163560019 Lab Value = 0.024 Expected Conc. = 0.024 Report level label = 0.01 Pct Recovery = 99% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl SpecificMix = 5054800 Laboratory ID = 20162150213 Lab Value = 0.020 Expected Conc. = 0.024 Report level label = 0.01 Pct Recovery = 83% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl SpecificMix = 5054800 Laboratory ID = 20173120093 Lab Value = 0.019 Expected Conc. = 0.021 Report level label = 0.01 Pct Recovery = 92% Analysis Date = 03/10/18 SpikeMix = ChemService 6472100: 30 µl & ChemService 6537100: 30 µl SpecificMix = 6472100 Laboratory ID = 20150150115 Lab Value = 0.014 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 68% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl SpecificMix = 032714 Laboratory ID = 20142820151 Lab Value = 0.019 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 95% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl SpecificMix = 032714 Laboratory ID = 20142470041 Lab Value = 0.021 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 102% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141910243 Lab Value = 0.019 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 92% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141640076 Lab Value = 0.021 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 103% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141490205 Lab Value = 0.020 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 101% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = 032714 Laboratory ID = 20141360094 Lab Value = 0.021 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 104% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141080004 Lab Value = 0.023 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 112% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl SpecificMix = 032714 Laboratory ID = 20161050143 Lab Value = 0.015 Expected Conc. = 0.015 Report level label = 0.01 Pct Recovery = 98% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Laboratory ID = 20160430111 Lab Value = 0.014 Expected Conc. = 0.015 Report level label = 0.01 Pct Recovery = 94% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Laboratory ID = 20160560044 Lab Value = 0.013 Expected Conc. = 0.015 Report level label = 0.01 Pct Recovery = 87% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl SpecificMix = EN150513008 Laboratory ID = 20160070059 Lab Value = 0.011 Expected Conc. = 0.015 Report level label = 0.01 Pct Recovery = 73% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = 040615 Laboratory ID = 20153160001 Lab Value = 0.015 Expected Conc. = 0.015 Report level label = 0.01 Pct Recovery = 97% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = EN150513008 Laboratory ID = 20153030068 Lab Value = 0.014 Expected Conc. = 0.015 Report level label = 0.01 Pct Recovery = 94% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150513008 Laboratory ID = 20152190003 Lab Value = 0.005 Expected Conc. = 0.015 Report level label = 0.01 Pct Recovery = 30% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150513008 Laboratory ID = 20151480170 Lab Value = 0.014 Expected Conc. = 0.015 Report level label = 0.01 Pct Recovery = 94% Analysis Date = 06/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150513008 Laboratory ID = 20151380009 Lab Value = 0.012 Expected Conc. = 0.015 Report level label = 0.01 Pct Recovery = 82% Analysis Date = 05/30/15 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Laboratory ID = 20151210037 Lab Value = 0.013 Expected Conc. = 0.015 Report level label = 0.01 Pct Recovery = 85% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Analysis Date = 03/10/18 Pct Recovery = 93% Analysis Date = 02/28/18 Pct Recovery = 93% Analysis Date = 02/28/18 Pct Recovery = 93% Analysis Date = 02/19/18 Pct Recovery = 93% Analysis Date = 02/19/18 Pct Recovery = 93% Analysis Date = 02/09/18 Pct Recovery = 92% Analysis Date = 02/09/18 Pct Recovery = 92% Analysis Date = 01/31/18 Pct Recovery = 92% Analysis Date = 01/31/18 Pct Recovery = 92% Analysis Date = 01/22/18 Pct Recovery = 92% Analysis Date = 01/22/18 Pct Recovery = 92% Analysis Date = 01/12/18 Pct Recovery = 92% Analysis Date = 01/12/18 Pct Recovery = 92% Analysis Date = 01/03/18 Pct Recovery = 92% Analysis Date = 01/03/18 Pct Recovery = 92% Analysis Date = 12/24/17 Pct Recovery = 92% Analysis Date = 12/24/17 Pct Recovery = 92% Analysis Date = 12/15/17 Pct Recovery = 92% Analysis Date = 12/15/17 Pct Recovery = 92% Analysis Date = 12/06/17 Pct Recovery = 92% Analysis Date = 12/06/17 Pct Recovery = 92% Analysis Date = 11/26/17 Pct Recovery = 91% Analysis Date = 11/26/17 Pct Recovery = 91% Analysis Date = 11/17/17 Pct Recovery = 91% Analysis Date = 11/17/17 Pct Recovery = 91% Analysis Date = 11/07/17 Pct Recovery = 91% Analysis Date = 11/07/17 Pct Recovery = 91% Analysis Date = 10/29/17 Pct Recovery = 91% Analysis Date = 10/29/17 Pct Recovery = 91% Analysis Date = 10/20/17 Pct Recovery = 91% Analysis Date = 10/20/17 Pct Recovery = 91% Analysis Date = 10/10/17 Pct Recovery = 91% Analysis Date = 10/10/17 Pct Recovery = 91% Analysis Date = 10/01/17 Pct Recovery = 91% Analysis Date = 10/01/17 Pct Recovery = 91% Analysis Date = 09/21/17 Pct Recovery = 91% Analysis Date = 09/21/17 Pct Recovery = 91% Analysis Date = 09/12/17 Pct Recovery = 90% Analysis Date = 09/12/17 Pct Recovery = 90% Analysis Date = 09/03/17 Pct Recovery = 90% Analysis Date = 09/03/17 Pct Recovery = 90% Analysis Date = 08/24/17 Pct Recovery = 90% Analysis Date = 08/24/17 Pct Recovery = 90% Analysis Date = 08/15/17 Pct Recovery = 90% Analysis Date = 08/15/17 Pct Recovery = 90% Analysis Date = 08/05/17 Pct Recovery = 90% Analysis Date = 08/05/17 Pct Recovery = 90% Analysis Date = 07/27/17 Pct Recovery = 90% Analysis Date = 07/27/17 Pct Recovery = 90% Analysis Date = 07/18/17 Pct Recovery = 90% Analysis Date = 07/18/17 Pct Recovery = 90% Analysis Date = 07/08/17 Pct Recovery = 89% Analysis Date = 07/08/17 Pct Recovery = 89% Analysis Date = 06/29/17 Pct Recovery = 89% Analysis Date = 06/29/17 Pct Recovery = 89% Analysis Date = 06/19/17 Pct Recovery = 89% Analysis Date = 06/19/17 Pct Recovery = 89% Analysis Date = 06/10/17 Pct Recovery = 89% Analysis Date = 06/10/17 Pct Recovery = 89% Analysis Date = 06/01/17 Pct Recovery = 89% Analysis Date = 06/01/17 Pct Recovery = 89% Analysis Date = 05/22/17 Pct Recovery = 89% Analysis Date = 05/22/17 Pct Recovery = 89% Analysis Date = 05/13/17 Pct Recovery = 89% Analysis Date = 05/13/17 Pct Recovery = 89% Analysis Date = 05/03/17 Pct Recovery = 89% Analysis Date = 05/03/17 Pct Recovery = 89% Analysis Date = 04/24/17 Pct Recovery = 88% Analysis Date = 04/24/17 Pct Recovery = 88% Analysis Date = 04/15/17 Pct Recovery = 88% Analysis Date = 04/15/17 Pct Recovery = 88% Analysis Date = 04/05/17 Pct Recovery = 88% Analysis Date = 04/05/17 Pct Recovery = 88% Analysis Date = 03/27/17 Pct Recovery = 88% Analysis Date = 03/27/17 Pct Recovery = 88% Analysis Date = 03/17/17 Pct Recovery = 88% Analysis Date = 03/17/17 Pct Recovery = 88% Analysis Date = 03/08/17 Pct Recovery = 88% Analysis Date = 03/08/17 Pct Recovery = 88% Analysis Date = 02/27/17 Pct Recovery = 88% Analysis Date = 02/27/17 Pct Recovery = 88% Analysis Date = 02/17/17 Pct Recovery = 88% Analysis Date = 02/17/17 Pct Recovery = 88% Analysis Date = 02/08/17 Pct Recovery = 87% Analysis Date = 02/08/17 Pct Recovery = 87% Analysis Date = 01/29/17 Pct Recovery = 87% Analysis Date = 01/29/17 Pct Recovery = 87% Analysis Date = 01/20/17 Pct Recovery = 87% Analysis Date = 01/20/17 Pct Recovery = 87% Analysis Date = 01/11/17 Pct Recovery = 87% Analysis Date = 01/11/17 Pct Recovery = 87% Analysis Date = 01/01/17 Pct Recovery = 87% Analysis Date = 01/01/17 Pct Recovery = 87% Analysis Date = 12/23/16 Pct Recovery = 87% Analysis Date = 12/23/16 Pct Recovery = 87% Analysis Date = 12/13/16 Pct Recovery = 87% Analysis Date = 12/13/16 Pct Recovery = 87% Analysis Date = 12/04/16 Pct Recovery = 86% Analysis Date = 12/04/16 Pct Recovery = 86% Analysis Date = 11/25/16 Pct Recovery = 86% Analysis Date = 11/25/16 Pct Recovery = 86% Analysis Date = 11/15/16 Pct Recovery = 86% Analysis Date = 11/15/16 Pct Recovery = 86% Analysis Date = 11/06/16 Pct Recovery = 86% Analysis Date = 11/06/16 Pct Recovery = 86% Analysis Date = 10/27/16 Pct Recovery = 86% Analysis Date = 10/27/16 Pct Recovery = 86% Analysis Date = 10/18/16 Pct Recovery = 86% Analysis Date = 10/18/16 Pct Recovery = 86% Analysis Date = 10/09/16 Pct Recovery = 86% Analysis Date = 10/09/16 Pct Recovery = 86% Analysis Date = 09/29/16 Pct Recovery = 85% Analysis Date = 09/29/16 Pct Recovery = 85% Analysis Date = 09/20/16 Pct Recovery = 85% Analysis Date = 09/20/16 Pct Recovery = 85% Analysis Date = 09/10/16 Pct Recovery = 85% Analysis Date = 09/10/16 Pct Recovery = 85% Analysis Date = 09/01/16 Pct Recovery = 85% Analysis Date = 09/01/16 Pct Recovery = 85% Analysis Date = 08/23/16 Pct Recovery = 85% Analysis Date = 08/23/16 Pct Recovery = 85% Analysis Date = 08/13/16 Pct Recovery = 85% Analysis Date = 08/13/16 Pct Recovery = 85% Analysis Date = 08/04/16 Pct Recovery = 84% Analysis Date = 08/04/16 Pct Recovery = 84% Analysis Date = 07/25/16 Pct Recovery = 84% Analysis Date = 07/25/16 Pct Recovery = 84% Analysis Date = 07/16/16 Pct Recovery = 84% Analysis Date = 07/16/16 Pct Recovery = 84% Analysis Date = 07/07/16 Pct Recovery = 84% Analysis Date = 07/07/16 Pct Recovery = 84% Analysis Date = 06/27/16 Pct Recovery = 84% Analysis Date = 06/27/16 Pct Recovery = 84% Analysis Date = 06/18/16 Pct Recovery = 84% Analysis Date = 06/18/16 Pct Recovery = 84% Analysis Date = 06/08/16 Pct Recovery = 83% Analysis Date = 06/08/16 Pct Recovery = 83% Analysis Date = 05/30/16 Pct Recovery = 83% Analysis Date = 05/30/16 Pct Recovery = 83% Analysis Date = 05/21/16 Pct Recovery = 83% Analysis Date = 05/21/16 Pct Recovery = 83% Analysis Date = 05/11/16 Pct Recovery = 83% Analysis Date = 05/11/16 Pct Recovery = 83% Analysis Date = 05/02/16 Pct Recovery = 83% Analysis Date = 05/02/16 Pct Recovery = 83% Analysis Date = 04/22/16 Pct Recovery = 83% Analysis Date = 04/22/16 Pct Recovery = 83% Analysis Date = 04/13/16 Pct Recovery = 82% Analysis Date = 04/13/16 Pct Recovery = 82% Analysis Date = 04/04/16 Pct Recovery = 82% Analysis Date = 04/04/16 Pct Recovery = 82% Analysis Date = 03/25/16 Pct Recovery = 82% Analysis Date = 03/25/16 Pct Recovery = 82% Analysis Date = 03/16/16 Pct Recovery = 82% Analysis Date = 03/16/16 Pct Recovery = 82% Analysis Date = 03/06/16 Pct Recovery = 82% Analysis Date = 03/06/16 Pct Recovery = 82% Analysis Date = 02/26/16 Pct Recovery = 82% Analysis Date = 02/26/16 Pct Recovery = 82% Analysis Date = 02/17/16 Pct Recovery = 82% Analysis Date = 02/17/16 Pct Recovery = 82% Analysis Date = 02/07/16 Pct Recovery = 81% Analysis Date = 02/07/16 Pct Recovery = 81% Analysis Date = 01/29/16 Pct Recovery = 81% Analysis Date = 01/29/16 Pct Recovery = 81% Analysis Date = 01/19/16 Pct Recovery = 81% Analysis Date = 01/19/16 Pct Recovery = 81% Analysis Date = 01/10/16 Pct Recovery = 81% Analysis Date = 01/10/16 Pct Recovery = 81% Analysis Date = 01/01/16 Pct Recovery = 81% Analysis Date = 01/01/16 Pct Recovery = 81% Analysis Date = 12/22/15 Pct Recovery = 81% Analysis Date = 12/22/15 Pct Recovery = 81% Analysis Date = 12/13/15 Pct Recovery = 82% Analysis Date = 12/13/15 Pct Recovery = 82% Analysis Date = 12/03/15 Pct Recovery = 82% Analysis Date = 12/03/15 Pct Recovery = 82% Analysis Date = 11/24/15 Pct Recovery = 82% Analysis Date = 11/24/15 Pct Recovery = 82% Analysis Date = 11/15/15 Pct Recovery = 82% Analysis Date = 11/15/15 Pct Recovery = 82% Analysis Date = 11/05/15 Pct Recovery = 82% Analysis Date = 11/05/15 Pct Recovery = 82% Analysis Date = 10/27/15 Pct Recovery = 82% Analysis Date = 10/27/15 Pct Recovery = 82% Analysis Date = 10/17/15 Pct Recovery = 82% Analysis Date = 10/17/15 Pct Recovery = 82% Analysis Date = 10/08/15 Pct Recovery = 82% Analysis Date = 10/08/15 Pct Recovery = 82% Analysis Date = 09/29/15 Pct Recovery = 82% Analysis Date = 09/29/15 Pct Recovery = 82% Analysis Date = 09/19/15 Pct Recovery = 82% Analysis Date = 09/19/15 Pct Recovery = 82% Analysis Date = 09/10/15 Pct Recovery = 82% Analysis Date = 09/10/15 Pct Recovery = 82% Analysis Date = 08/31/15 Pct Recovery = 82% Analysis Date = 08/31/15 Pct Recovery = 82% Analysis Date = 08/22/15 Pct Recovery = 82% Analysis Date = 08/22/15 Pct Recovery = 82% Analysis Date = 08/13/15 Pct Recovery = 82% Analysis Date = 08/13/15 Pct Recovery = 82% Analysis Date = 08/03/15 Pct Recovery = 83% Analysis Date = 08/03/15 Pct Recovery = 83% Analysis Date = 07/25/15 Pct Recovery = 83% Analysis Date = 07/25/15 Pct Recovery = 83% Analysis Date = 07/15/15 Pct Recovery = 83% Analysis Date = 07/15/15 Pct Recovery = 83% Analysis Date = 07/06/15 Pct Recovery = 83% Analysis Date = 07/06/15 Pct Recovery = 83% Analysis Date = 06/27/15 Pct Recovery = 83% Analysis Date = 06/27/15 Pct Recovery = 83% Analysis Date = 06/17/15 Pct Recovery = 83% Analysis Date = 06/17/15 Pct Recovery = 83% Analysis Date = 06/08/15 Pct Recovery = 83% Analysis Date = 06/08/15 Pct Recovery = 83% Analysis Date = 05/29/15 Pct Recovery = 83% Analysis Date = 05/29/15 Pct Recovery = 83% Analysis Date = 05/20/15 Pct Recovery = 84% Analysis Date = 05/20/15 Pct Recovery = 84% Analysis Date = 05/11/15 Pct Recovery = 84% Analysis Date = 05/11/15 Pct Recovery = 84% Analysis Date = 05/01/15 Pct Recovery = 84% Analysis Date = 05/01/15 Pct Recovery = 84% Analysis Date = 04/22/15 Pct Recovery = 84% Analysis Date = 04/22/15 Pct Recovery = 84% Analysis Date = 04/12/15 Pct Recovery = 85% Analysis Date = 04/12/15 Pct Recovery = 85% Analysis Date = 04/03/15 Pct Recovery = 85% Analysis Date = 04/03/15 Pct Recovery = 85% Analysis Date = 03/25/15 Pct Recovery = 85% Analysis Date = 03/25/15 Pct Recovery = 85% Analysis Date = 03/15/15 Pct Recovery = 85% Analysis Date = 03/15/15 Pct Recovery = 85% Analysis Date = 03/06/15 Pct Recovery = 86% Analysis Date = 03/06/15 Pct Recovery = 86% Analysis Date = 02/24/15 Pct Recovery = 86% Analysis Date = 02/24/15 Pct Recovery = 86% Analysis Date = 02/15/15 Pct Recovery = 86% Analysis Date = 02/15/15 Pct Recovery = 86% Analysis Date = 02/06/15 Pct Recovery = 86% Analysis Date = 02/06/15 Pct Recovery = 86% Analysis Date = 01/27/15 Pct Recovery = 87% Analysis Date = 01/27/15 Pct Recovery = 87% Analysis Date = 01/18/15 Pct Recovery = 87% Analysis Date = 01/18/15 Pct Recovery = 87% Analysis Date = 01/08/15 Pct Recovery = 87% Analysis Date = 01/08/15 Pct Recovery = 87% Analysis Date = 12/30/14 Pct Recovery = 87% Analysis Date = 12/30/14 Pct Recovery = 87% Analysis Date = 12/21/14 Pct Recovery = 88% Analysis Date = 12/21/14 Pct Recovery = 88% Analysis Date = 12/11/14 Pct Recovery = 88% Analysis Date = 12/11/14 Pct Recovery = 88% Analysis Date = 12/02/14 Pct Recovery = 88% Analysis Date = 12/02/14 Pct Recovery = 88% Analysis Date = 11/22/14 Pct Recovery = 88% Analysis Date = 11/22/14 Pct Recovery = 88% Analysis Date = 11/13/14 Pct Recovery = 89% Analysis Date = 11/13/14 Pct Recovery = 89% Analysis Date = 11/04/14 Pct Recovery = 89% Analysis Date = 11/04/14 Pct Recovery = 89% Analysis Date = 10/25/14 Pct Recovery = 89% Analysis Date = 10/25/14 Pct Recovery = 89% Analysis Date = 10/16/14 Pct Recovery = 90% Analysis Date = 10/16/14 Pct Recovery = 90% Analysis Date = 10/06/14 Pct Recovery = 90% Analysis Date = 10/06/14 Pct Recovery = 90% Analysis Date = 09/27/14 Pct Recovery = 90% Analysis Date = 09/27/14 Pct Recovery = 90% Analysis Date = 09/18/14 Pct Recovery = 91% Analysis Date = 09/18/14 Pct Recovery = 91% Analysis Date = 09/08/14 Pct Recovery = 91% Analysis Date = 09/08/14 Pct Recovery = 91% Analysis Date = 08/30/14 Pct Recovery = 92% Analysis Date = 08/30/14 Pct Recovery = 92% Analysis Date = 08/20/14 Pct Recovery = 92% Analysis Date = 08/20/14 Pct Recovery = 92% Analysis Date = 08/11/14 Pct Recovery = 93% Analysis Date = 08/11/14 Pct Recovery = 93% Analysis Date = 08/02/14 Pct Recovery = 93% Analysis Date = 08/02/14 Pct Recovery = 93% Analysis Date = 07/23/14 Pct Recovery = 93% Analysis Date = 07/23/14 Pct Recovery = 93% Analysis Date = 07/14/14 Pct Recovery = 94% Analysis Date = 07/14/14 Pct Recovery = 94% Analysis Date = 07/04/14 Pct Recovery = 94% Analysis Date = 07/04/14 Pct Recovery = 94% Analysis Date = 06/25/14 Pct Recovery = 94% Analysis Date = 06/25/14 Pct Recovery = 94% Analysis Date = 06/16/14 Pct Recovery = 94% Analysis Date = 06/16/14 Pct Recovery = 94% Analysis Date = 06/06/14 Pct Recovery = 95% Analysis Date = 06/06/14 Pct Recovery = 95% Analysis Date = 05/28/14 Pct Recovery = 95% Analysis Date = 05/28/14 Pct Recovery = 95% Analysis Date = 05/18/14 Pct Recovery = 95% Analysis Date = 05/18/14 Pct Recovery = 95% Analysis Date = 05/09/14 Pct Recovery = 95% Analysis Date = 05/09/14 Pct Recovery = 95% Analysis Date = 04/30/14 Pct Recovery = 95% Analysis Date = 04/30/14 Pct Recovery = 95% Analysis Date = 04/20/14 Pct Recovery = 95% Analysis Date = 04/20/14 Pct Recovery = 95% Analysis Date = 04/11/14 Pct Recovery = 95% Analysis Date = 04/11/14 Pct Recovery = 95% Analysis Date = 04/01/14 Pct Recovery = 95% Analysis Date = 04/01/14 Pct Recovery = 95% Analysis Date = 03/23/14 Pct Recovery = 95% Analysis Date = 03/23/14 Pct Recovery = 95% Analysis Date = 03/14/14 Pct Recovery = 96% Analysis Date = 03/14/14 Pct Recovery = 96% Analysis Date = 03/04/14 Pct Recovery = 96% Analysis Date = 03/04/14 Pct Recovery = 96% Analysis Date = 02/23/14 Pct Recovery = 96% Analysis Date = 02/23/14 Pct Recovery = 96% Analysis Date = 02/13/14 Pct Recovery = 96% Analysis Date = 02/13/14 Pct Recovery = 96% Analysis Date = 02/04/14 Pct Recovery = 96% Analysis Date = 02/04/14 Pct Recovery = 96% Analysis Date = 01/26/14 Pct Recovery = 96% Analysis Date = 01/26/14 Pct Recovery = 96% Analysis Date = 01/16/14 Pct Recovery = 96% Analysis Date = 01/16/14 Pct Recovery = 96% Analysis Date = 01/07/14 Pct Recovery = 96% Analysis Date = 01/07/14 Pct Recovery = 96% Analysis Date = 12/28/13 Pct Recovery = 96% Analysis Date = 12/28/13 Pct Recovery = 96% Analysis Date = 12/19/13 Pct Recovery = 96% Analysis Date = 12/19/13 Pct Recovery = 96% Analysis Date = 12/10/13 Pct Recovery = 96% Analysis Date = 12/10/13 Pct Recovery = 96% Analysis Date = 11/30/13 Pct Recovery = 96% Analysis Date = 11/30/13 Pct Recovery = 96% Analysis Date = 11/21/13 Pct Recovery = 97% Analysis Date = 11/21/13 Pct Recovery = 97% Analysis Date = 11/11/13 Pct Recovery = 97% Analysis Date = 11/11/13 Pct Recovery = 97% Analysis Date = 11/02/13 Pct Recovery = 97% Analysis Date = 11/02/13 Pct Recovery = 97% Analysis Date = 10/24/13 Pct Recovery = 97% Analysis Date = 10/24/13 Pct Recovery = 97% Analysis Date = 10/14/13 Pct Recovery = 97% Analysis Date = 10/14/13 Pct Recovery = 97% Analysis Date = 10/05/13 Pct Recovery = 97% Analysis Date = 10/05/13 Pct Recovery = 97% Analysis Date = 09/25/13 Pct Recovery = 97% Analysis Date = 09/25/13 Pct Recovery = 97% Analysis Date = 09/16/13 Pct Recovery = 97% Analysis Date = 09/16/13 Pct Recovery = 97% Analysis Date = 09/07/13 Pct Recovery = 97% Analysis Date = 09/07/13 Pct Recovery = 97% Analysis Date = 08/28/13 Pct Recovery = 97% Analysis Date = 08/28/13 Pct Recovery = 97% Analysis Date = 08/19/13 Pct Recovery = 97% Analysis Date = 08/19/13 Pct Recovery = 97% Analysis Date = 08/09/13 Pct Recovery = 97% Analysis Date = 08/09/13 Pct Recovery = 97% Analysis Date = 07/31/13 Pct Recovery = 97% Analysis Date = 07/31/13 Pct Recovery = 97% Analysis Date = 07/22/13 Pct Recovery = 97% Analysis Date = 07/22/13 Pct Recovery = 97% Analysis Date = 07/12/13 Pct Recovery = 97% Analysis Date = 07/12/13 Pct Recovery = 97% Analysis Date = 07/03/13 Pct Recovery = 97% Analysis Date = 07/03/13 Pct Recovery = 97% Analysis Date = 06/23/13 Pct Recovery = 97% Analysis Date = 06/23/13 Pct Recovery = 97% Analysis Date = 06/14/13 Pct Recovery = 97% Analysis Date = 06/14/13 Pct Recovery = 97% Analysis Date = 06/05/13 Pct Recovery = 97% Analysis Date = 06/05/13 Pct Recovery = 97% Analysis Date = 05/26/13 Pct Recovery = 97% Analysis Date = 05/26/13 Pct Recovery = 97% Analysis Date = 05/17/13 Pct Recovery = 97% Analysis Date = 05/17/13 Pct Recovery = 97% Analysis Date = 05/07/13 Pct Recovery = 97% Analysis Date = 05/07/13 Pct Recovery = 97% Analysis Date = 04/28/13 Pct Recovery = 97% Analysis Date = 04/28/13 Pct Recovery = 97% Analysis Date = 04/19/13 Pct Recovery = 97% Analysis Date = 04/19/13 Pct Recovery = 97% Analysis Date = 04/09/13 Pct Recovery = 97% Analysis Date = 04/09/13 Pct Recovery = 97% Analysis Date = 03/31/13 Pct Recovery = 97% Analysis Date = 03/31/13 Pct Recovery = 97% Analysis Date = 03/21/13 Pct Recovery = 97% Analysis Date = 03/21/13 Pct Recovery = 97% Analysis Date = 03/12/13 Pct Recovery = 97% Analysis Date = 03/12/13 Pct Recovery = 97% Analysis Date = 03/03/13 Pct Recovery = 97% Analysis Date = 03/03/13 Pct Recovery = 97% Analysis Date = 02/21/13 Pct Recovery = 97% Analysis Date = 02/21/13 Pct Recovery = 97% Analysis Date = 02/12/13 Pct Recovery = 97% Analysis Date = 02/12/13 Pct Recovery = 97% Analysis Date = 02/02/13 Pct Recovery = 97% Analysis Date = 02/02/13 Pct Recovery = 97% Analysis Date = 01/24/13 Pct Recovery = 97% Analysis Date = 01/24/13 Pct Recovery = 97% Analysis Date = 01/15/13 Pct Recovery = 97% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
2-ETHYL-6-METHYLANILINE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 68 89% 15% 91% 11%
Total 68 89% 15% 91% 11%

Sample Statistics
2-ETHYL-6-METHYLANILINE

Characteristic N % % Basis
Plotted 68 99% Spiked
Estimated Values 68 99% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 69 .  
False Negatives 1 1% 1 out of 69
Not Spiked 46 .  
False Positives 0 0% 0 out of 46

OBSP Determination:
3,4-DICHLOROANILINE
METHOD: 2033 , TESTIDCODE: 61625GCM39

Laboratory ID = 20130250061 Lab Value = 0.059 Expected Conc. = 0.1 Report level label = 0.006 Pct Recovery = 59% Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl SpecificMix = A088380 Laboratory ID = 20140100085 Lab Value = 0.072 Expected Conc. = 0.09 Report level label = 0.006 Pct Recovery = 80% Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl SpecificMix = T1130514013 Laboratory ID = 20132490342 Lab Value = 0.069 Expected Conc. = 0.09 Report level label = 0.006 Pct Recovery = 77% Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl SpecificMix = T1130514013 Laboratory ID = 20140230082 Lab Value = 0.034 Expected Conc. = 0.05 Report level label = 0.006 Pct Recovery = 67% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl SpecificMix = A093651 Laboratory ID = 20132420001 Lab Value = 0.043 Expected Conc. = 0.05 Report level label = 0.006 Pct Recovery = 85% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl SpecificMix = A093651 Laboratory ID = 20130810108 Lab Value = 0.047 Expected Conc. = 0.05 Report level label = 0.006 Pct Recovery = 94% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl SpecificMix = T1120530013 Laboratory ID = 20123560092 Lab Value = 0.036 Expected Conc. = 0.05 Report level label = 0.006 Pct Recovery = 71% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = T1120530013 Laboratory ID = 20140370077 Lab Value = 0.031 Expected Conc. = 0.045 Report level label = 0.006 Pct Recovery = 69% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl SpecificMix = T1130514013 Laboratory ID = 20132690010 Lab Value = 0.041 Expected Conc. = 0.045 Report level label = 0.006 Pct Recovery = 90% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl SpecificMix = T1130514013 Laboratory ID = 20131370001 Lab Value = 0.038 Expected Conc. = 0.045 Report level label = 0.006 Pct Recovery = 85% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl SpecificMix = 1473000 Laboratory ID = 20162860079 Lab Value = 0.035 Expected Conc. = 0.038 Report level label = 0.006 Pct Recovery = 92% Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl SpecificMix = 060916 Laboratory ID = 20163150006 Lab Value = 0.025 Expected Conc. = 0.038 Report level label = 0.006 Pct Recovery = 66% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl SpecificMix = 060916 Laboratory ID = 20152610011 Lab Value = 0.022 Expected Conc. = 0.0362 Report level label = 0.006 Pct Recovery = 60% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl SpecificMix = 0406-15-01 Laboratory ID = 20152460215 Lab Value = 0.025 Expected Conc. = 0.0362 Report level label = 0.006 Pct Recovery = 69% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl SpecificMix = 0406-15-01 Laboratory ID = 20171660002 Lab Value = 0.024 Expected Conc. = 0.0304 Report level label = 0.006 Pct Recovery = 80% Analysis Date = 08/23/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = 060916 Laboratory ID = 20171380001 Lab Value = 0.017 Expected Conc. = 0.0304 Report level label = 0.006 Pct Recovery = 55% Analysis Date = 06/07/17 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 041816 Laboratory ID = 20170740063 Lab Value = 0.019 Expected Conc. = 0.0304 Report level label = 0.006 Pct Recovery = 61% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl SpecificMix = 041816 Laboratory ID = 20170190026 Lab Value = 0.020 Expected Conc. = 0.0304 Report level label = 0.006 Pct Recovery = 67% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = 060916 Laboratory ID = 20161740258 Lab Value = 0.016 Expected Conc. = 0.0304 Report level label = 0.006 Pct Recovery = 51% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 041816 Laboratory ID = 20150720069 Lab Value = 0.013 Expected Conc. = 0.024 Report level label = 0.006 Pct Recovery = 54% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 03DD006 Laboratory ID = 20143110108 Lab Value = 0.017 Expected Conc. = 0.024 Report level label = 0.006 Pct Recovery = 72% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 03DD006 Laboratory ID = 20142960086 Lab Value = 0.016 Expected Conc. = 0.024 Report level label = 0.006 Pct Recovery = 66% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 03DD006 Laboratory ID = 20142720002 Lab Value = 0.014 Expected Conc. = 0.024 Report level label = 0.006 Pct Recovery = 57% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl SpecificMix = LC06435 Laboratory ID = 20142530087 Lab Value = 0.014 Expected Conc. = 0.024 Report level label = 0.006 Pct Recovery = 57% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl SpecificMix = LC06435 Laboratory ID = 20142270001 Lab Value = 0.016 Expected Conc. = 0.024 Report level label = 0.006 Pct Recovery = 67% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl SpecificMix = 03DD006 Laboratory ID = 20141570088 Lab Value = 0.020 Expected Conc. = 0.024 Report level label = 0.006 Pct Recovery = 85% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl SpecificMix = LC06435 Laboratory ID = 20141220025 Lab Value = 0.018 Expected Conc. = 0.024 Report level label = 0.006 Pct Recovery = 74% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl SpecificMix = LC06435 Laboratory ID = 20172560101 Lab Value = 0.013 Expected Conc. = 0.02 Report level label = 0.006 Pct Recovery = 63% Analysis Date = 12/22/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6567600: 50 µl SpecificMix = EN170808006 Laboratory ID = 20172370001 Lab Value = 0.016 Expected Conc. = 0.02 Report level label = 0.006 Pct Recovery = 78% Analysis Date = 11/18/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6537100: 50 µl SpecificMix = EN170808006 Laboratory ID = 20172230001 Lab Value = 0.017 Expected Conc. = 0.02 Report level label = 0.006 Pct Recovery = 85% Analysis Date = 10/19/17 SpikeMix = ChemService 6472100: 50 µl & Abs 071717Pest: 50 µl SpecificMix = 6472100 Laboratory ID = 20161260151 Lab Value = 0.014 Expected Conc. = 0.02 Report level label = 0.006 Pct Recovery = 71% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = 3851600 Laboratory ID = 20151550293 Lab Value = 0.014 Expected Conc. = 0.02 Report level label = 0.006 Pct Recovery = 72% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl SpecificMix = 3851600 Laboratory ID = 20151270112 Lab Value = 0.014 Expected Conc. = 0.02 Report level label = 0.006 Pct Recovery = 70% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl SpecificMix = 3851600 Laboratory ID = 20140860102 Lab Value = 0.013 Expected Conc. = 0.02 Report level label = 0.006 Pct Recovery = 66% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl SpecificMix = A093651 Laboratory ID = 20133400002 Lab Value = 0.016 Expected Conc. = 0.02 Report level label = 0.006 Pct Recovery = 81% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = A093651 Laboratory ID = 20132910008 Lab Value = 0.015 Expected Conc. = 0.02 Report level label = 0.006 Pct Recovery = 75% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = A093651 Laboratory ID = 20131920149 Lab Value = 0.017 Expected Conc. = 0.02 Report level label = 0.006 Pct Recovery = 83% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl SpecificMix = A093651 Laboratory ID = 20131230084 Lab Value = 0.020 Expected Conc. = 0.02 Report level label = 0.006 Pct Recovery = 101% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl SpecificMix = A088380 Laboratory ID = 20130650005 Lab Value = 0.013 Expected Conc. = 0.02 Report level label = 0.006 Pct Recovery = 66% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl SpecificMix = A088380 Laboratory ID = 20130390105 Lab Value = 0.018 Expected Conc. = 0.02 Report level label = 0.006 Pct Recovery = 88% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl SpecificMix = T1120530013 Laboratory ID = 20160770090 Lab Value = 0.013 Expected Conc. = 0.0181 Report level label = 0.006 Pct Recovery = 70% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20160630046 Lab Value = 0.013 Expected Conc. = 0.0181 Report level label = 0.006 Pct Recovery = 71% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20153510109 Lab Value = 0.011 Expected Conc. = 0.0181 Report level label = 0.006 Pct Recovery = 62% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20153440001 Lab Value = 0.011 Expected Conc. = 0.0181 Report level label = 0.006 Pct Recovery = 62% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20140730138 Lab Value = 0.011 Expected Conc. = 0.018 Report level label = 0.006 Pct Recovery = 61% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 1473000 Laboratory ID = 20133470008 Lab Value = 0.015 Expected Conc. = 0.018 Report level label = 0.006 Pct Recovery = 83% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl SpecificMix = 1473000 Laboratory ID = 20133310030 Lab Value = 0.014 Expected Conc. = 0.018 Report level label = 0.006 Pct Recovery = 77% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl SpecificMix = 1473000 Laboratory ID = 20133050050 Lab Value = 0.017 Expected Conc. = 0.018 Report level label = 0.006 Pct Recovery = 94% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl SpecificMix = T1130514013 Laboratory ID = 20132280016 Lab Value = 0.018 Expected Conc. = 0.018 Report level label = 0.006 Pct Recovery = 100% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl SpecificMix = T1130514013 Laboratory ID = 20131790009 Lab Value = 0.016 Expected Conc. = 0.018 Report level label = 0.006 Pct Recovery = 91% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl SpecificMix = 1473000 Laboratory ID = 20131650073 Lab Value = 0.013 Expected Conc. = 0.018 Report level label = 0.006 Pct Recovery = 74% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl SpecificMix = 1473000 Laboratory ID = 20171940002 Lab Value = 0.013 Expected Conc. = 0.0152 Report level label = 0.006 Pct Recovery = 84% Analysis Date = 11/10/17 SpikeMix = ChemService 5054800: 40 µl & NSI 041816: 40 µl SpecificMix = 041816 Laboratory ID = 20171160110 Lab Value = 0.011 Expected Conc. = 0.0152 Report level label = 0.006 Pct Recovery = 70% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = 060916 Laboratory ID = 20162520001 Lab Value = 0.014 Expected Conc. = 0.0152 Report level label = 0.006 Pct Recovery = 89% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl SpecificMix = 060916 Laboratory ID = 20163560019 Lab Value = 0.012 Expected Conc. = 0.0152 Report level label = 0.006 Pct Recovery = 80% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl SpecificMix = 060916 Laboratory ID = 20162380004 Lab Value = 0.013 Expected Conc. = 0.0152 Report level label = 0.006 Pct Recovery = 88% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = 060916 Laboratory ID = 20162020124 Lab Value = 0.012 Expected Conc. = 0.0152 Report level label = 0.006 Pct Recovery = 79% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl SpecificMix = 041816 Laboratory ID = 20161600087 Lab Value = 0.010 Expected Conc. = 0.0152 Report level label = 0.006 Pct Recovery = 65% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 041816 Laboratory ID = 20161340228 Lab Value = 0.011 Expected Conc. = 0.0152 Report level label = 0.006 Pct Recovery = 74% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl SpecificMix = 041816 Laboratory ID = 20161190075 Lab Value = 0.011 Expected Conc. = 0.0152 Report level label = 0.006 Pct Recovery = 75% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 041816 Laboratory ID = 20173120093 Lab Value = 0.011 Expected Conc. = 0.012 Report level label = 0.006 Pct Recovery = 88% Analysis Date = 03/10/18 SpikeMix = ChemService 6472100: 30 µl & ChemService 6537100: 30 µl SpecificMix = 6472100 Laboratory ID = 20150150115 Lab Value = 0.008 Expected Conc. = 0.012 Report level label = 0.006 Pct Recovery = 64% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl SpecificMix = LC06435 Laboratory ID = 20143370094 Lab Value = 0.007 Expected Conc. = 0.012 Report level label = 0.006 Pct Recovery = 59% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl SpecificMix = LC06435 Laboratory ID = 20142200164 Lab Value = 0.009 Expected Conc. = 0.012 Report level label = 0.006 Pct Recovery = 77% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 03DD006 Laboratory ID = 20141910243 Lab Value = 0.008 Expected Conc. = 0.012 Report level label = 0.006 Pct Recovery = 67% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = LC06435 Laboratory ID = 20141840097 Lab Value = 0.007 Expected Conc. = 0.012 Report level label = 0.006 Pct Recovery = 58% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl SpecificMix = LC06435 Laboratory ID = 20141640076 Lab Value = 0.011 Expected Conc. = 0.012 Report level label = 0.006 Pct Recovery = 88% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = 03DD006 Laboratory ID = 20141420140 Lab Value = 0.005 Expected Conc. = 0.012 Report level label = 0.006 Pct Recovery = 45% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 03DD006 Laboratory ID = 20141080004 Lab Value = 0.009 Expected Conc. = 0.012 Report level label = 0.006 Pct Recovery = 76% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl SpecificMix = 03DD006 Laboratory ID = 20160430111 Lab Value = 0.008 Expected Conc. = 0.01 Report level label = 0.006 Pct Recovery = 84% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 3851600 Laboratory ID = 20160210080 Lab Value = 0.007 Expected Conc. = 0.01 Report level label = 0.006 Pct Recovery = 70% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 3851600 Laboratory ID = 20152950078 Lab Value = 0.006 Expected Conc. = 0.01 Report level label = 0.006 Pct Recovery = 57% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 3851600 Laboratory ID = 20153030068 Lab Value = 0.008 Expected Conc. = 0.01 Report level label = 0.006 Pct Recovery = 81% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = 3851600 Laboratory ID = 20151760208 Lab Value = 0.006 Expected Conc. = 0.01 Report level label = 0.006 Pct Recovery = 58% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl SpecificMix = 3851600 Laboratory ID = 20151380009 Lab Value = 0.006 Expected Conc. = 0.01 Report level label = 0.006 Pct Recovery = 58% Analysis Date = 05/30/15 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 3851600 Laboratory ID = 20152190003 Lab Value = 0.005 Expected Conc. = 0.0091 Report level label = 0.006 Pct Recovery = 58% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = 0406-15-01 Laboratory ID = 20152040177 Lab Value = 0.006 Expected Conc. = 0.0091 Report level label = 0.006 Pct Recovery = 68% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl SpecificMix = 0406-15-01 Analysis Date = 03/10/18 Pct Recovery = 80% Analysis Date = 02/28/18 Pct Recovery = 80% Analysis Date = 02/28/18 Pct Recovery = 80% Analysis Date = 02/19/18 Pct Recovery = 80% Analysis Date = 02/19/18 Pct Recovery = 80% Analysis Date = 02/09/18 Pct Recovery = 79% Analysis Date = 02/09/18 Pct Recovery = 79% Analysis Date = 01/31/18 Pct Recovery = 79% Analysis Date = 01/31/18 Pct Recovery = 79% Analysis Date = 01/22/18 Pct Recovery = 79% Analysis Date = 01/22/18 Pct Recovery = 79% Analysis Date = 01/12/18 Pct Recovery = 79% Analysis Date = 01/12/18 Pct Recovery = 79% Analysis Date = 01/03/18 Pct Recovery = 79% Analysis Date = 01/03/18 Pct Recovery = 79% Analysis Date = 12/24/17 Pct Recovery = 79% Analysis Date = 12/24/17 Pct Recovery = 79% Analysis Date = 12/15/17 Pct Recovery = 79% Analysis Date = 12/15/17 Pct Recovery = 79% Analysis Date = 12/06/17 Pct Recovery = 78% Analysis Date = 12/06/17 Pct Recovery = 78% Analysis Date = 11/26/17 Pct Recovery = 78% Analysis Date = 11/26/17 Pct Recovery = 78% Analysis Date = 11/17/17 Pct Recovery = 78% Analysis Date = 11/17/17 Pct Recovery = 78% Analysis Date = 11/07/17 Pct Recovery = 78% Analysis Date = 11/07/17 Pct Recovery = 78% Analysis Date = 10/29/17 Pct Recovery = 78% Analysis Date = 10/29/17 Pct Recovery = 78% Analysis Date = 10/20/17 Pct Recovery = 78% Analysis Date = 10/20/17 Pct Recovery = 78% Analysis Date = 10/10/17 Pct Recovery = 78% Analysis Date = 10/10/17 Pct Recovery = 78% Analysis Date = 10/01/17 Pct Recovery = 77% Analysis Date = 10/01/17 Pct Recovery = 77% Analysis Date = 09/21/17 Pct Recovery = 77% Analysis Date = 09/21/17 Pct Recovery = 77% Analysis Date = 09/12/17 Pct Recovery = 77% Analysis Date = 09/12/17 Pct Recovery = 77% Analysis Date = 09/03/17 Pct Recovery = 77% Analysis Date = 09/03/17 Pct Recovery = 77% Analysis Date = 08/24/17 Pct Recovery = 77% Analysis Date = 08/24/17 Pct Recovery = 77% Analysis Date = 08/15/17 Pct Recovery = 77% Analysis Date = 08/15/17 Pct Recovery = 77% Analysis Date = 08/05/17 Pct Recovery = 77% Analysis Date = 08/05/17 Pct Recovery = 77% Analysis Date = 07/27/17 Pct Recovery = 76% Analysis Date = 07/27/17 Pct Recovery = 76% Analysis Date = 07/18/17 Pct Recovery = 76% Analysis Date = 07/18/17 Pct Recovery = 76% Analysis Date = 07/08/17 Pct Recovery = 76% Analysis Date = 07/08/17 Pct Recovery = 76% Analysis Date = 06/29/17 Pct Recovery = 76% Analysis Date = 06/29/17 Pct Recovery = 76% Analysis Date = 06/19/17 Pct Recovery = 76% Analysis Date = 06/19/17 Pct Recovery = 76% Analysis Date = 06/10/17 Pct Recovery = 76% Analysis Date = 06/10/17 Pct Recovery = 76% Analysis Date = 06/01/17 Pct Recovery = 76% Analysis Date = 06/01/17 Pct Recovery = 76% Analysis Date = 05/22/17 Pct Recovery = 75% Analysis Date = 05/22/17 Pct Recovery = 75% Analysis Date = 05/13/17 Pct Recovery = 75% Analysis Date = 05/13/17 Pct Recovery = 75% Analysis Date = 05/03/17 Pct Recovery = 75% Analysis Date = 05/03/17 Pct Recovery = 75% Analysis Date = 04/24/17 Pct Recovery = 75% Analysis Date = 04/24/17 Pct Recovery = 75% Analysis Date = 04/15/17 Pct Recovery = 75% Analysis Date = 04/15/17 Pct Recovery = 75% Analysis Date = 04/05/17 Pct Recovery = 75% Analysis Date = 04/05/17 Pct Recovery = 75% Analysis Date = 03/27/17 Pct Recovery = 75% Analysis Date = 03/27/17 Pct Recovery = 75% Analysis Date = 03/17/17 Pct Recovery = 74% Analysis Date = 03/17/17 Pct Recovery = 74% Analysis Date = 03/08/17 Pct Recovery = 74% Analysis Date = 03/08/17 Pct Recovery = 74% Analysis Date = 02/27/17 Pct Recovery = 74% Analysis Date = 02/27/17 Pct Recovery = 74% Analysis Date = 02/17/17 Pct Recovery = 74% Analysis Date = 02/17/17 Pct Recovery = 74% Analysis Date = 02/08/17 Pct Recovery = 74% Analysis Date = 02/08/17 Pct Recovery = 74% Analysis Date = 01/29/17 Pct Recovery = 74% Analysis Date = 01/29/17 Pct Recovery = 74% Analysis Date = 01/20/17 Pct Recovery = 74% Analysis Date = 01/20/17 Pct Recovery = 74% Analysis Date = 01/11/17 Pct Recovery = 73% Analysis Date = 01/11/17 Pct Recovery = 73% Analysis Date = 01/01/17 Pct Recovery = 73% Analysis Date = 01/01/17 Pct Recovery = 73% Analysis Date = 12/23/16 Pct Recovery = 73% Analysis Date = 12/23/16 Pct Recovery = 73% Analysis Date = 12/13/16 Pct Recovery = 73% Analysis Date = 12/13/16 Pct Recovery = 73% Analysis Date = 12/04/16 Pct Recovery = 73% Analysis Date = 12/04/16 Pct Recovery = 73% Analysis Date = 11/25/16 Pct Recovery = 73% Analysis Date = 11/25/16 Pct Recovery = 73% Analysis Date = 11/15/16 Pct Recovery = 72% Analysis Date = 11/15/16 Pct Recovery = 72% Analysis Date = 11/06/16 Pct Recovery = 72% Analysis Date = 11/06/16 Pct Recovery = 72% Analysis Date = 10/27/16 Pct Recovery = 72% Analysis Date = 10/27/16 Pct Recovery = 72% Analysis Date = 10/18/16 Pct Recovery = 72% Analysis Date = 10/18/16 Pct Recovery = 72% Analysis Date = 10/09/16 Pct Recovery = 72% Analysis Date = 10/09/16 Pct Recovery = 72% Analysis Date = 09/29/16 Pct Recovery = 72% Analysis Date = 09/29/16 Pct Recovery = 72% Analysis Date = 09/20/16 Pct Recovery = 72% Analysis Date = 09/20/16 Pct Recovery = 72% Analysis Date = 09/10/16 Pct Recovery = 71% Analysis Date = 09/10/16 Pct Recovery = 71% Analysis Date = 09/01/16 Pct Recovery = 71% Analysis Date = 09/01/16 Pct Recovery = 71% Analysis Date = 08/23/16 Pct Recovery = 71% Analysis Date = 08/23/16 Pct Recovery = 71% Analysis Date = 08/13/16 Pct Recovery = 71% Analysis Date = 08/13/16 Pct Recovery = 71% Analysis Date = 08/04/16 Pct Recovery = 71% Analysis Date = 08/04/16 Pct Recovery = 71% Analysis Date = 07/25/16 Pct Recovery = 71% Analysis Date = 07/25/16 Pct Recovery = 71% Analysis Date = 07/16/16 Pct Recovery = 71% Analysis Date = 07/16/16 Pct Recovery = 71% Analysis Date = 07/07/16 Pct Recovery = 70% Analysis Date = 07/07/16 Pct Recovery = 70% Analysis Date = 06/27/16 Pct Recovery = 70% Analysis Date = 06/27/16 Pct Recovery = 70% Analysis Date = 06/18/16 Pct Recovery = 70% Analysis Date = 06/18/16 Pct Recovery = 70% Analysis Date = 06/08/16 Pct Recovery = 70% Analysis Date = 06/08/16 Pct Recovery = 70% Analysis Date = 05/30/16 Pct Recovery = 70% Analysis Date = 05/30/16 Pct Recovery = 70% Analysis Date = 05/21/16 Pct Recovery = 70% Analysis Date = 05/21/16 Pct Recovery = 70% Analysis Date = 05/11/16 Pct Recovery = 70% Analysis Date = 05/11/16 Pct Recovery = 70% Analysis Date = 05/02/16 Pct Recovery = 69% Analysis Date = 05/02/16 Pct Recovery = 69% Analysis Date = 04/22/16 Pct Recovery = 69% Analysis Date = 04/22/16 Pct Recovery = 69% Analysis Date = 04/13/16 Pct Recovery = 69% Analysis Date = 04/13/16 Pct Recovery = 69% Analysis Date = 04/04/16 Pct Recovery = 69% Analysis Date = 04/04/16 Pct Recovery = 69% Analysis Date = 03/25/16 Pct Recovery = 69% Analysis Date = 03/25/16 Pct Recovery = 69% Analysis Date = 03/16/16 Pct Recovery = 69% Analysis Date = 03/16/16 Pct Recovery = 69% Analysis Date = 03/06/16 Pct Recovery = 69% Analysis Date = 03/06/16 Pct Recovery = 69% Analysis Date = 02/26/16 Pct Recovery = 68% Analysis Date = 02/26/16 Pct Recovery = 68% Analysis Date = 02/17/16 Pct Recovery = 68% Analysis Date = 02/17/16 Pct Recovery = 68% Analysis Date = 02/07/16 Pct Recovery = 68% Analysis Date = 02/07/16 Pct Recovery = 68% Analysis Date = 01/29/16 Pct Recovery = 68% Analysis Date = 01/29/16 Pct Recovery = 68% Analysis Date = 01/19/16 Pct Recovery = 68% Analysis Date = 01/19/16 Pct Recovery = 68% Analysis Date = 01/10/16 Pct Recovery = 68% Analysis Date = 01/10/16 Pct Recovery = 68% Analysis Date = 01/01/16 Pct Recovery = 68% Analysis Date = 01/01/16 Pct Recovery = 68% Analysis Date = 12/22/15 Pct Recovery = 68% Analysis Date = 12/22/15 Pct Recovery = 68% Analysis Date = 12/13/15 Pct Recovery = 68% Analysis Date = 12/13/15 Pct Recovery = 68% Analysis Date = 12/03/15 Pct Recovery = 67% Analysis Date = 12/03/15 Pct Recovery = 67% Analysis Date = 11/24/15 Pct Recovery = 67% Analysis Date = 11/24/15 Pct Recovery = 67% Analysis Date = 11/15/15 Pct Recovery = 67% Analysis Date = 11/15/15 Pct Recovery = 67% Analysis Date = 11/05/15 Pct Recovery = 67% Analysis Date = 11/05/15 Pct Recovery = 67% Analysis Date = 10/27/15 Pct Recovery = 67% Analysis Date = 10/27/15 Pct Recovery = 67% Analysis Date = 10/17/15 Pct Recovery = 67% Analysis Date = 10/17/15 Pct Recovery = 67% Analysis Date = 10/08/15 Pct Recovery = 67% Analysis Date = 10/08/15 Pct Recovery = 67% Analysis Date = 09/29/15 Pct Recovery = 67% Analysis Date = 09/29/15 Pct Recovery = 67% Analysis Date = 09/19/15 Pct Recovery = 67% Analysis Date = 09/19/15 Pct Recovery = 67% Analysis Date = 09/10/15 Pct Recovery = 67% Analysis Date = 09/10/15 Pct Recovery = 67% Analysis Date = 08/31/15 Pct Recovery = 67% Analysis Date = 08/31/15 Pct Recovery = 67% Analysis Date = 08/22/15 Pct Recovery = 66% Analysis Date = 08/22/15 Pct Recovery = 66% Analysis Date = 08/13/15 Pct Recovery = 66% Analysis Date = 08/13/15 Pct Recovery = 66% Analysis Date = 08/03/15 Pct Recovery = 66% Analysis Date = 08/03/15 Pct Recovery = 66% Analysis Date = 07/25/15 Pct Recovery = 66% Analysis Date = 07/25/15 Pct Recovery = 66% Analysis Date = 07/15/15 Pct Recovery = 66% Analysis Date = 07/15/15 Pct Recovery = 66% Analysis Date = 07/06/15 Pct Recovery = 66% Analysis Date = 07/06/15 Pct Recovery = 66% Analysis Date = 06/27/15 Pct Recovery = 66% Analysis Date = 06/27/15 Pct Recovery = 66% Analysis Date = 06/17/15 Pct Recovery = 66% Analysis Date = 06/17/15 Pct Recovery = 66% Analysis Date = 06/08/15 Pct Recovery = 66% Analysis Date = 06/08/15 Pct Recovery = 66% Analysis Date = 05/29/15 Pct Recovery = 66% Analysis Date = 05/29/15 Pct Recovery = 66% Analysis Date = 05/20/15 Pct Recovery = 66% Analysis Date = 05/20/15 Pct Recovery = 66% Analysis Date = 05/11/15 Pct Recovery = 66% Analysis Date = 05/11/15 Pct Recovery = 66% Analysis Date = 05/01/15 Pct Recovery = 66% Analysis Date = 05/01/15 Pct Recovery = 66% Analysis Date = 04/22/15 Pct Recovery = 66% Analysis Date = 04/22/15 Pct Recovery = 66% Analysis Date = 04/12/15 Pct Recovery = 66% Analysis Date = 04/12/15 Pct Recovery = 66% Analysis Date = 04/03/15 Pct Recovery = 66% Analysis Date = 04/03/15 Pct Recovery = 66% Analysis Date = 03/25/15 Pct Recovery = 65% Analysis Date = 03/25/15 Pct Recovery = 65% Analysis Date = 03/15/15 Pct Recovery = 65% Analysis Date = 03/15/15 Pct Recovery = 65% Analysis Date = 03/06/15 Pct Recovery = 65% Analysis Date = 03/06/15 Pct Recovery = 65% Analysis Date = 02/24/15 Pct Recovery = 65% Analysis Date = 02/24/15 Pct Recovery = 65% Analysis Date = 02/15/15 Pct Recovery = 65% Analysis Date = 02/15/15 Pct Recovery = 65% Analysis Date = 02/06/15 Pct Recovery = 65% Analysis Date = 02/06/15 Pct Recovery = 65% Analysis Date = 01/27/15 Pct Recovery = 65% Analysis Date = 01/27/15 Pct Recovery = 65% Analysis Date = 01/18/15 Pct Recovery = 66% Analysis Date = 01/18/15 Pct Recovery = 66% Analysis Date = 01/08/15 Pct Recovery = 66% Analysis Date = 01/08/15 Pct Recovery = 66% Analysis Date = 12/30/14 Pct Recovery = 66% Analysis Date = 12/30/14 Pct Recovery = 66% Analysis Date = 12/21/14 Pct Recovery = 66% Analysis Date = 12/21/14 Pct Recovery = 66% Analysis Date = 12/11/14 Pct Recovery = 66% Analysis Date = 12/11/14 Pct Recovery = 66% Analysis Date = 12/02/14 Pct Recovery = 67% Analysis Date = 12/02/14 Pct Recovery = 67% Analysis Date = 11/22/14 Pct Recovery = 67% Analysis Date = 11/22/14 Pct Recovery = 67% Analysis Date = 11/13/14 Pct Recovery = 67% Analysis Date = 11/13/14 Pct Recovery = 67% Analysis Date = 11/04/14 Pct Recovery = 67% Analysis Date = 11/04/14 Pct Recovery = 67% Analysis Date = 10/25/14 Pct Recovery = 67% Analysis Date = 10/25/14 Pct Recovery = 67% Analysis Date = 10/16/14 Pct Recovery = 68% Analysis Date = 10/16/14 Pct Recovery = 68% Analysis Date = 10/06/14 Pct Recovery = 68% Analysis Date = 10/06/14 Pct Recovery = 68% Analysis Date = 09/27/14 Pct Recovery = 68% Analysis Date = 09/27/14 Pct Recovery = 68% Analysis Date = 09/18/14 Pct Recovery = 68% Analysis Date = 09/18/14 Pct Recovery = 68% Analysis Date = 09/08/14 Pct Recovery = 69% Analysis Date = 09/08/14 Pct Recovery = 69% Analysis Date = 08/30/14 Pct Recovery = 69% Analysis Date = 08/30/14 Pct Recovery = 69% Analysis Date = 08/20/14 Pct Recovery = 69% Analysis Date = 08/20/14 Pct Recovery = 69% Analysis Date = 08/11/14 Pct Recovery = 69% Analysis Date = 08/11/14 Pct Recovery = 69% Analysis Date = 08/02/14 Pct Recovery = 69% Analysis Date = 08/02/14 Pct Recovery = 69% Analysis Date = 07/23/14 Pct Recovery = 70% Analysis Date = 07/23/14 Pct Recovery = 70% Analysis Date = 07/14/14 Pct Recovery = 70% Analysis Date = 07/14/14 Pct Recovery = 70% Analysis Date = 07/04/14 Pct Recovery = 70% Analysis Date = 07/04/14 Pct Recovery = 70% Analysis Date = 06/25/14 Pct Recovery = 71% Analysis Date = 06/25/14 Pct Recovery = 71% Analysis Date = 06/16/14 Pct Recovery = 71% Analysis Date = 06/16/14 Pct Recovery = 71% Analysis Date = 06/06/14 Pct Recovery = 71% Analysis Date = 06/06/14 Pct Recovery = 71% Analysis Date = 05/28/14 Pct Recovery = 72% Analysis Date = 05/28/14 Pct Recovery = 72% Analysis Date = 05/18/14 Pct Recovery = 72% Analysis Date = 05/18/14 Pct Recovery = 72% Analysis Date = 05/09/14 Pct Recovery = 72% Analysis Date = 05/09/14 Pct Recovery = 72% Analysis Date = 04/30/14 Pct Recovery = 73% Analysis Date = 04/30/14 Pct Recovery = 73% Analysis Date = 04/20/14 Pct Recovery = 73% Analysis Date = 04/20/14 Pct Recovery = 73% Analysis Date = 04/11/14 Pct Recovery = 73% Analysis Date = 04/11/14 Pct Recovery = 73% Analysis Date = 04/01/14 Pct Recovery = 73% Analysis Date = 04/01/14 Pct Recovery = 73% Analysis Date = 03/23/14 Pct Recovery = 74% Analysis Date = 03/23/14 Pct Recovery = 74% Analysis Date = 03/14/14 Pct Recovery = 74% Analysis Date = 03/14/14 Pct Recovery = 74% Analysis Date = 03/04/14 Pct Recovery = 74% Analysis Date = 03/04/14 Pct Recovery = 74% Analysis Date = 02/23/14 Pct Recovery = 75% Analysis Date = 02/23/14 Pct Recovery = 75% Analysis Date = 02/13/14 Pct Recovery = 75% Analysis Date = 02/13/14 Pct Recovery = 75% Analysis Date = 02/04/14 Pct Recovery = 75% Analysis Date = 02/04/14 Pct Recovery = 75% Analysis Date = 01/26/14 Pct Recovery = 76% Analysis Date = 01/26/14 Pct Recovery = 76% Analysis Date = 01/16/14 Pct Recovery = 76% Analysis Date = 01/16/14 Pct Recovery = 76% Analysis Date = 01/07/14 Pct Recovery = 76% Analysis Date = 01/07/14 Pct Recovery = 76% Analysis Date = 12/28/13 Pct Recovery = 77% Analysis Date = 12/28/13 Pct Recovery = 77% Analysis Date = 12/19/13 Pct Recovery = 77% Analysis Date = 12/19/13 Pct Recovery = 77% Analysis Date = 12/10/13 Pct Recovery = 77% Analysis Date = 12/10/13 Pct Recovery = 77% Analysis Date = 11/30/13 Pct Recovery = 77% Analysis Date = 11/30/13 Pct Recovery = 77% Analysis Date = 11/21/13 Pct Recovery = 78% Analysis Date = 11/21/13 Pct Recovery = 78% Analysis Date = 11/11/13 Pct Recovery = 78% Analysis Date = 11/11/13 Pct Recovery = 78% Analysis Date = 11/02/13 Pct Recovery = 78% Analysis Date = 11/02/13 Pct Recovery = 78% Analysis Date = 10/24/13 Pct Recovery = 78% Analysis Date = 10/24/13 Pct Recovery = 78% Analysis Date = 10/14/13 Pct Recovery = 79% Analysis Date = 10/14/13 Pct Recovery = 79% Analysis Date = 10/05/13 Pct Recovery = 79% Analysis Date = 10/05/13 Pct Recovery = 79% Analysis Date = 09/25/13 Pct Recovery = 79% Analysis Date = 09/25/13 Pct Recovery = 79% Analysis Date = 09/16/13 Pct Recovery = 79% Analysis Date = 09/16/13 Pct Recovery = 79% Analysis Date = 09/07/13 Pct Recovery = 80% Analysis Date = 09/07/13 Pct Recovery = 80% Analysis Date = 08/28/13 Pct Recovery = 80% Analysis Date = 08/28/13 Pct Recovery = 80% Analysis Date = 08/19/13 Pct Recovery = 80% Analysis Date = 08/19/13 Pct Recovery = 80% Analysis Date = 08/09/13 Pct Recovery = 80% Analysis Date = 08/09/13 Pct Recovery = 80% Analysis Date = 07/31/13 Pct Recovery = 81% Analysis Date = 07/31/13 Pct Recovery = 81% Analysis Date = 07/22/13 Pct Recovery = 81% Analysis Date = 07/22/13 Pct Recovery = 81% Analysis Date = 07/12/13 Pct Recovery = 81% Analysis Date = 07/12/13 Pct Recovery = 81% Analysis Date = 07/03/13 Pct Recovery = 81% Analysis Date = 07/03/13 Pct Recovery = 81% Analysis Date = 06/23/13 Pct Recovery = 82% Analysis Date = 06/23/13 Pct Recovery = 82% Analysis Date = 06/14/13 Pct Recovery = 82% Analysis Date = 06/14/13 Pct Recovery = 82% Analysis Date = 06/05/13 Pct Recovery = 82% Analysis Date = 06/05/13 Pct Recovery = 82% Analysis Date = 05/26/13 Pct Recovery = 82% Analysis Date = 05/26/13 Pct Recovery = 82% Analysis Date = 05/17/13 Pct Recovery = 83% Analysis Date = 05/17/13 Pct Recovery = 83% Analysis Date = 05/07/13 Pct Recovery = 83% Analysis Date = 05/07/13 Pct Recovery = 83% Analysis Date = 04/28/13 Pct Recovery = 83% Analysis Date = 04/28/13 Pct Recovery = 83% Analysis Date = 04/19/13 Pct Recovery = 83% Analysis Date = 04/19/13 Pct Recovery = 83% Analysis Date = 04/09/13 Pct Recovery = 84% Analysis Date = 04/09/13 Pct Recovery = 84% Analysis Date = 03/31/13 Pct Recovery = 84% Analysis Date = 03/31/13 Pct Recovery = 84% Analysis Date = 03/21/13 Pct Recovery = 84% Analysis Date = 03/21/13 Pct Recovery = 84% Analysis Date = 03/12/13 Pct Recovery = 84% Analysis Date = 03/12/13 Pct Recovery = 84% Analysis Date = 03/03/13 Pct Recovery = 85% Analysis Date = 03/03/13 Pct Recovery = 85% Analysis Date = 02/21/13 Pct Recovery = 85% Analysis Date = 02/21/13 Pct Recovery = 85% Analysis Date = 02/12/13 Pct Recovery = 85% Analysis Date = 02/12/13 Pct Recovery = 85% Analysis Date = 02/02/13 Pct Recovery = 85% Analysis Date = 02/02/13 Pct Recovery = 85% Analysis Date = 01/24/13 Pct Recovery = 86% Analysis Date = 01/24/13 Pct Recovery = 86% Analysis Date = 01/15/13 Pct Recovery = 86% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
3,4-DICHLOROANILINE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 77 73% 12% 71% 14%
Total 77 73% 12% 71% 14%

Sample Statistics
3,4-DICHLOROANILINE

Characteristic N % % Basis
Plotted 77 100% Spiked
Estimated Values 77 100% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 77 .  
False Negatives 0 0% 0 out of 77
Not Spiked 41 .  
False Positives 0 0% 0 out of 41

OBSP Determination:
3,5-DICHLOROANILINE
METHOD: 2033 , TESTIDCODE: 61627GCM39

Laboratory ID = 20130250061 Lab Value = 0.114 Expected Conc. = 0.15 Report level label = 0.006 Pct Recovery = 76% Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl SpecificMix = A088380 Laboratory ID = 20140100085 Lab Value = 0.107 Expected Conc. = 0.12 Report level label = 0.006 Pct Recovery = 89% Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl SpecificMix = T1130514013 Laboratory ID = 20132490342 Lab Value = 0.098 Expected Conc. = 0.12 Report level label = 0.006 Pct Recovery = 82% Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl SpecificMix = T1130514013 Laboratory ID = 20140230082 Lab Value = 0.059 Expected Conc. = 0.075 Report level label = 0.006 Pct Recovery = 79% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl SpecificMix = A093651 Laboratory ID = 20132420001 Lab Value = 0.067 Expected Conc. = 0.075 Report level label = 0.006 Pct Recovery = 89% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl SpecificMix = A093651 Laboratory ID = 20130810108 Lab Value = 0.074 Expected Conc. = 0.075 Report level label = 0.006 Pct Recovery = 98% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl SpecificMix = T1120530013 Laboratory ID = 20123560092 Lab Value = 0.064 Expected Conc. = 0.075 Report level label = 0.006 Pct Recovery = 86% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = T1120530013 Laboratory ID = 20131370001 Lab Value = 0.062 Expected Conc. = 0.063 Report level label = 0.006 Pct Recovery = 98% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl SpecificMix = 1473000 Laboratory ID = 20140370077 Lab Value = 0.046 Expected Conc. = 0.06 Report level label = 0.006 Pct Recovery = 77% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl SpecificMix = T1130514013 Laboratory ID = 20132690010 Lab Value = 0.054 Expected Conc. = 0.06 Report level label = 0.006 Pct Recovery = 90% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl SpecificMix = T1130514013 Laboratory ID = 20180390003 Lab Value = 0.026 Expected Conc. = 0.04 Report level label = 0.008 Pct Recovery = 64% Analysis Date = 04/06/18 SpikeMix = Spex Organics EN170808006: 100 µl & Abs 071717Pest: 100 µl SpecificMix = 071717Pest Laboratory ID = 20172510330 Lab Value = 0.035 Expected Conc. = 0.04 Report level label = 0.006 Pct Recovery = 87% Analysis Date = 12/29/17 SpikeMix = ChemService 6537100: 100 µl & Abs 071817Pest: 100 µl SpecificMix = 6537100 Laboratory ID = 20162860079 Lab Value = 0.041 Expected Conc. = 0.04 Report level label = 0.006 Pct Recovery = 104% Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl SpecificMix = 5054800 Laboratory ID = 20161880109 Lab Value = 0.037 Expected Conc. = 0.04 Report level label = 0.006 Pct Recovery = 92% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl SpecificMix = 5054800 Laboratory ID = 20163370001 Lab Value = 0.035 Expected Conc. = 0.0375 Report level label = 0.006 Pct Recovery = 93% Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl SpecificMix = LC20138V Laboratory ID = 20152750006 Lab Value = 0.026 Expected Conc. = 0.036 Report level label = 0.006 Pct Recovery = 71% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl SpecificMix = EN150514012 Laboratory ID = 20152460215 Lab Value = 0.032 Expected Conc. = 0.036 Report level label = 0.006 Pct Recovery = 88% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl SpecificMix = EN150514012 Laboratory ID = 20171380001 Lab Value = 0.023 Expected Conc. = 0.032 Report level label = 0.006 Pct Recovery = 73% Analysis Date = 06/07/17 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 5054800 Laboratory ID = 20170960001 Lab Value = 0.026 Expected Conc. = 0.032 Report level label = 0.006 Pct Recovery = 82% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl SpecificMix = 5054800 Laboratory ID = 20161740258 Lab Value = 0.022 Expected Conc. = 0.032 Report level label = 0.006 Pct Recovery = 69% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 5054800 Laboratory ID = 20171720140 Lab Value = 0.026 Expected Conc. = 0.03 Report level label = 0.006 Pct Recovery = 87% Analysis Date = 08/31/17 SpikeMix = Supelco LC20138V: 80 µl & Phenova B20160331: 80 µl SpecificMix = LC20138V Laboratory ID = 20170740063 Lab Value = 0.023 Expected Conc. = 0.03 Report level label = 0.006 Pct Recovery = 76% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl SpecificMix = LC20138V Laboratory ID = 20161470001 Lab Value = 0.027 Expected Conc. = 0.03 Report level label = 0.006 Pct Recovery = 88% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl SpecificMix = LC20138V Laboratory ID = 20140860102 Lab Value = 0.024 Expected Conc. = 0.03 Report level label = 0.006 Pct Recovery = 80% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl SpecificMix = A093651 Laboratory ID = 20133400002 Lab Value = 0.028 Expected Conc. = 0.03 Report level label = 0.006 Pct Recovery = 94% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = A093651 Laboratory ID = 20132910008 Lab Value = 0.024 Expected Conc. = 0.03 Report level label = 0.006 Pct Recovery = 79% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = A093651 Laboratory ID = 20131920149 Lab Value = 0.026 Expected Conc. = 0.03 Report level label = 0.006 Pct Recovery = 88% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl SpecificMix = A093651 Laboratory ID = 20131230084 Lab Value = 0.031 Expected Conc. = 0.03 Report level label = 0.006 Pct Recovery = 103% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl SpecificMix = A088380 Laboratory ID = 20130650005 Lab Value = 0.024 Expected Conc. = 0.03 Report level label = 0.006 Pct Recovery = 79% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl SpecificMix = A088380 Laboratory ID = 20130390105 Lab Value = 0.027 Expected Conc. = 0.03 Report level label = 0.006 Pct Recovery = 91% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl SpecificMix = T1120530013 Laboratory ID = 20140730138 Lab Value = 0.018 Expected Conc. = 0.0252 Report level label = 0.006 Pct Recovery = 73% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 1473000 Laboratory ID = 20133470008 Lab Value = 0.024 Expected Conc. = 0.0252 Report level label = 0.006 Pct Recovery = 93% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl SpecificMix = 1473000 Laboratory ID = 20133310030 Lab Value = 0.024 Expected Conc. = 0.0252 Report level label = 0.006 Pct Recovery = 96% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl SpecificMix = 1473000 Laboratory ID = 20131790009 Lab Value = 0.024 Expected Conc. = 0.0252 Report level label = 0.006 Pct Recovery = 94% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl SpecificMix = 1473000 Laboratory ID = 20131650073 Lab Value = 0.022 Expected Conc. = 0.0252 Report level label = 0.006 Pct Recovery = 89% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl SpecificMix = 1473000 Laboratory ID = 20142720002 Lab Value = 0.018 Expected Conc. = 0.0241 Report level label = 0.006 Pct Recovery = 73% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl SpecificMix = LC06435 Laboratory ID = 20142530087 Lab Value = 0.018 Expected Conc. = 0.0241 Report level label = 0.006 Pct Recovery = 73% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl SpecificMix = LC06435 Laboratory ID = 20141570088 Lab Value = 0.025 Expected Conc. = 0.0241 Report level label = 0.006 Pct Recovery = 104% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl SpecificMix = LC06435 Laboratory ID = 20141220025 Lab Value = 0.023 Expected Conc. = 0.0241 Report level label = 0.006 Pct Recovery = 93% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl SpecificMix = LC06435 Laboratory ID = 20150720069 Lab Value = 0.017 Expected Conc. = 0.024 Report level label = 0.006 Pct Recovery = 69% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 03DD006 Laboratory ID = 20143110108 Lab Value = 0.020 Expected Conc. = 0.024 Report level label = 0.006 Pct Recovery = 83% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 03DD006 Laboratory ID = 20142960086 Lab Value = 0.019 Expected Conc. = 0.024 Report level label = 0.006 Pct Recovery = 81% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 03DD006 Laboratory ID = 20142270001 Lab Value = 0.020 Expected Conc. = 0.024 Report level label = 0.006 Pct Recovery = 83% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl SpecificMix = 03DD006 Laboratory ID = 20133050050 Lab Value = 0.023 Expected Conc. = 0.024 Report level label = 0.006 Pct Recovery = 95% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl SpecificMix = T1130514013 Laboratory ID = 20132280016 Lab Value = 0.023 Expected Conc. = 0.024 Report level label = 0.006 Pct Recovery = 97% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl SpecificMix = T1130514013 Laboratory ID = 20173480003 Lab Value = 0.018 Expected Conc. = 0.02 Report level label = 0.008 Pct Recovery = 91% Analysis Date = 04/05/18 SpikeMix = Abs 071717Pest: 50 µl & ChemService 6567600: 50 µl SpecificMix = 071717Pest Laboratory ID = 20172370001 Lab Value = 0.018 Expected Conc. = 0.02 Report level label = 0.006 Pct Recovery = 89% Analysis Date = 11/18/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6537100: 50 µl SpecificMix = 6537100 Laboratory ID = 20172230001 Lab Value = 0.020 Expected Conc. = 0.02 Report level label = 0.006 Pct Recovery = 101% Analysis Date = 10/19/17 SpikeMix = ChemService 6472100: 50 µl & Abs 071717Pest: 50 µl SpecificMix = 071717Pest Laboratory ID = 20153440001 Lab Value = 0.014 Expected Conc. = 0.018 Report level label = 0.006 Pct Recovery = 76% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = EN150514012 Laboratory ID = 20152330039 Lab Value = 0.017 Expected Conc. = 0.018 Report level label = 0.006 Pct Recovery = 94% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl SpecificMix = 041415 Laboratory ID = 20151900132 Lab Value = 0.015 Expected Conc. = 0.018 Report level label = 0.006 Pct Recovery = 84% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl SpecificMix = 041415 Laboratory ID = 20151270112 Lab Value = 0.015 Expected Conc. = 0.018 Report level label = 0.006 Pct Recovery = 83% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl SpecificMix = 041415 Laboratory ID = 20171940002 Lab Value = 0.016 Expected Conc. = 0.016 Report level label = 0.006 Pct Recovery = 99% Analysis Date = 11/10/17 SpikeMix = ChemService 5054800: 40 µl & NSI 041816: 40 µl SpecificMix = 5054800 Laboratory ID = 20172020035 Lab Value = 0.016 Expected Conc. = 0.016 Report level label = 0.006 Pct Recovery = 100% Analysis Date = 11/07/17 SpikeMix = Abs 071717Pest: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 071717Pest Laboratory ID = 20170460061 Lab Value = 0.012 Expected Conc. = 0.016 Report level label = 0.006 Pct Recovery = 77% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl SpecificMix = 5054800 Laboratory ID = 20163560019 Lab Value = 0.015 Expected Conc. = 0.016 Report level label = 0.006 Pct Recovery = 92% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl SpecificMix = 5054800 Laboratory ID = 20162150213 Lab Value = 0.013 Expected Conc. = 0.016 Report level label = 0.006 Pct Recovery = 82% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl SpecificMix = 5054800 Laboratory ID = 20171510080 Lab Value = 0.014 Expected Conc. = 0.015 Report level label = 0.006 Pct Recovery = 94% Analysis Date = 06/09/17 SpikeMix = Supelco LC20138V: 40 µl & Crescent 03FF076: 40 µl SpecificMix = LC20138V Laboratory ID = 20162520001 Lab Value = 0.016 Expected Conc. = 0.015 Report level label = 0.006 Pct Recovery = 107% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl SpecificMix = LC20138V Laboratory ID = 20162660005 Lab Value = 0.013 Expected Conc. = 0.015 Report level label = 0.006 Pct Recovery = 87% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl SpecificMix = LC20138V Laboratory ID = 20162020124 Lab Value = 0.014 Expected Conc. = 0.015 Report level label = 0.006 Pct Recovery = 95% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl SpecificMix = LC20138V Laboratory ID = 20150150115 Lab Value = 0.010 Expected Conc. = 0.0121 Report level label = 0.006 Pct Recovery = 79% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl SpecificMix = LC06435 Laboratory ID = 20143370094 Lab Value = 0.009 Expected Conc. = 0.0121 Report level label = 0.006 Pct Recovery = 72% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl SpecificMix = LC06435 Laboratory ID = 20141910243 Lab Value = 0.010 Expected Conc. = 0.0121 Report level label = 0.006 Pct Recovery = 79% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = LC06435 Laboratory ID = 20141840097 Lab Value = 0.009 Expected Conc. = 0.0121 Report level label = 0.006 Pct Recovery = 74% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl SpecificMix = LC06435 Laboratory ID = 20180940080 Lab Value = 0.010 Expected Conc. = 0.012 Report level label = 0.008 Pct Recovery = 83% Analysis Date = 05/31/18 SpikeMix = ChemService 6472100: 30 µl & Abs 071717Pest: 30 µl SpecificMix = 071717Pest Laboratory ID = 20180730064 Lab Value = 0.012 Expected Conc. = 0.012 Report level label = 0.008 Pct Recovery = 100% Analysis Date = 05/16/18 SpikeMix = Abs 071717Pest: 30 µl & Abs 071817Pest: 30 µl SpecificMix = 071717Pest Laboratory ID = 20173120093 Lab Value = 0.012 Expected Conc. = 0.012 Report level label = 0.006 Pct Recovery = 97% Analysis Date = 03/10/18 SpikeMix = ChemService 6472100: 30 µl & ChemService 6537100: 30 µl SpecificMix = 6537100 Laboratory ID = 20172780018 Lab Value = 0.010 Expected Conc. = 0.012 Report level label = 0.006 Pct Recovery = 79% Analysis Date = 02/08/18 SpikeMix = ChemService 6537100: 30 µl & Abs 071817Pest: 30 µl SpecificMix = 6537100 Laboratory ID = 20142200164 Lab Value = 0.011 Expected Conc. = 0.012 Report level label = 0.006 Pct Recovery = 93% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 03DD006 Laboratory ID = 20141640076 Lab Value = 0.012 Expected Conc. = 0.012 Report level label = 0.006 Pct Recovery = 98% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = 03DD006 Laboratory ID = 20141420140 Lab Value = 0.007 Expected Conc. = 0.012 Report level label = 0.006 Pct Recovery = 62% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 03DD006 Laboratory ID = 20141080004 Lab Value = 0.011 Expected Conc. = 0.012 Report level label = 0.006 Pct Recovery = 90% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl SpecificMix = 03DD006 Laboratory ID = 20160560044 Lab Value = 0.009 Expected Conc. = 0.009 Report level label = 0.006 Pct Recovery = 96% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl SpecificMix = 041415 Laboratory ID = 20160070059 Lab Value = 0.008 Expected Conc. = 0.009 Report level label = 0.006 Pct Recovery = 93% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = EN150514012 Laboratory ID = 20153160001 Lab Value = 0.009 Expected Conc. = 0.009 Report level label = 0.006 Pct Recovery = 94% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = EN150514012 Laboratory ID = 20152950078 Lab Value = 0.006 Expected Conc. = 0.009 Report level label = 0.006 Pct Recovery = 67% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 041415 Laboratory ID = 20151760208 Lab Value = 0.007 Expected Conc. = 0.009 Report level label = 0.006 Pct Recovery = 73% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl SpecificMix = EN150514012 Laboratory ID = 20151480170 Lab Value = 0.008 Expected Conc. = 0.009 Report level label = 0.006 Pct Recovery = 86% Analysis Date = 06/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150514012 Laboratory ID = 20151210037 Lab Value = 0.008 Expected Conc. = 0.009 Report level label = 0.006 Pct Recovery = 83% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 041415 Analysis Date = 05/31/18 Pct Recovery = 90% Analysis Date = 05/21/18 Pct Recovery = 90% Analysis Date = 05/21/18 Pct Recovery = 90% Analysis Date = 05/11/18 Pct Recovery = 90% Analysis Date = 05/11/18 Pct Recovery = 90% Analysis Date = 05/01/18 Pct Recovery = 90% Analysis Date = 05/01/18 Pct Recovery = 90% Analysis Date = 04/21/18 Pct Recovery = 90% Analysis Date = 04/21/18 Pct Recovery = 90% Analysis Date = 04/11/18 Pct Recovery = 90% Analysis Date = 04/11/18 Pct Recovery = 90% Analysis Date = 04/02/18 Pct Recovery = 90% Analysis Date = 04/02/18 Pct Recovery = 90% Analysis Date = 03/23/18 Pct Recovery = 90% Analysis Date = 03/23/18 Pct Recovery = 90% Analysis Date = 03/13/18 Pct Recovery = 90% Analysis Date = 03/13/18 Pct Recovery = 90% Analysis Date = 03/03/18 Pct Recovery = 90% Analysis Date = 03/03/18 Pct Recovery = 90% Analysis Date = 02/21/18 Pct Recovery = 90% Analysis Date = 02/21/18 Pct Recovery = 90% Analysis Date = 02/12/18 Pct Recovery = 90% Analysis Date = 02/12/18 Pct Recovery = 90% Analysis Date = 02/02/18 Pct Recovery = 89% Analysis Date = 02/02/18 Pct Recovery = 89% Analysis Date = 01/23/18 Pct Recovery = 89% Analysis Date = 01/23/18 Pct Recovery = 89% Analysis Date = 01/13/18 Pct Recovery = 89% Analysis Date = 01/13/18 Pct Recovery = 89% Analysis Date = 01/03/18 Pct Recovery = 89% Analysis Date = 01/03/18 Pct Recovery = 89% Analysis Date = 12/25/17 Pct Recovery = 89% Analysis Date = 12/25/17 Pct Recovery = 89% Analysis Date = 12/15/17 Pct Recovery = 89% Analysis Date = 12/15/17 Pct Recovery = 89% Analysis Date = 12/05/17 Pct Recovery = 89% Analysis Date = 12/05/17 Pct Recovery = 89% Analysis Date = 11/25/17 Pct Recovery = 89% Analysis Date = 11/25/17 Pct Recovery = 89% Analysis Date = 11/15/17 Pct Recovery = 89% Analysis Date = 11/15/17 Pct Recovery = 89% Analysis Date = 11/05/17 Pct Recovery = 89% Analysis Date = 11/05/17 Pct Recovery = 89% Analysis Date = 10/27/17 Pct Recovery = 89% Analysis Date = 10/27/17 Pct Recovery = 89% Analysis Date = 10/17/17 Pct Recovery = 89% Analysis Date = 10/17/17 Pct Recovery = 89% Analysis Date = 10/07/17 Pct Recovery = 89% Analysis Date = 10/07/17 Pct Recovery = 89% Analysis Date = 09/27/17 Pct Recovery = 89% Analysis Date = 09/27/17 Pct Recovery = 89% Analysis Date = 09/17/17 Pct Recovery = 89% Analysis Date = 09/17/17 Pct Recovery = 89% Analysis Date = 09/08/17 Pct Recovery = 89% Analysis Date = 09/08/17 Pct Recovery = 89% Analysis Date = 08/29/17 Pct Recovery = 89% Analysis Date = 08/29/17 Pct Recovery = 89% Analysis Date = 08/19/17 Pct Recovery = 89% Analysis Date = 08/19/17 Pct Recovery = 89% Analysis Date = 08/09/17 Pct Recovery = 89% Analysis Date = 08/09/17 Pct Recovery = 89% Analysis Date = 07/30/17 Pct Recovery = 88% Analysis Date = 07/30/17 Pct Recovery = 88% Analysis Date = 07/21/17 Pct Recovery = 88% Analysis Date = 07/21/17 Pct Recovery = 88% Analysis Date = 07/11/17 Pct Recovery = 88% Analysis Date = 07/11/17 Pct Recovery = 88% Analysis Date = 07/01/17 Pct Recovery = 88% Analysis Date = 07/01/17 Pct Recovery = 88% Analysis Date = 06/21/17 Pct Recovery = 88% Analysis Date = 06/21/17 Pct Recovery = 88% Analysis Date = 06/11/17 Pct Recovery = 88% Analysis Date = 06/11/17 Pct Recovery = 88% Analysis Date = 06/02/17 Pct Recovery = 88% Analysis Date = 06/02/17 Pct Recovery = 88% Analysis Date = 05/23/17 Pct Recovery = 88% Analysis Date = 05/23/17 Pct Recovery = 88% Analysis Date = 05/13/17 Pct Recovery = 88% Analysis Date = 05/13/17 Pct Recovery = 88% Analysis Date = 05/03/17 Pct Recovery = 88% Analysis Date = 05/03/17 Pct Recovery = 88% Analysis Date = 04/23/17 Pct Recovery = 88% Analysis Date = 04/23/17 Pct Recovery = 88% Analysis Date = 04/13/17 Pct Recovery = 88% Analysis Date = 04/13/17 Pct Recovery = 88% Analysis Date = 04/04/17 Pct Recovery = 88% Analysis Date = 04/04/17 Pct Recovery = 88% Analysis Date = 03/25/17 Pct Recovery = 88% Analysis Date = 03/25/17 Pct Recovery = 88% Analysis Date = 03/15/17 Pct Recovery = 88% Analysis Date = 03/15/17 Pct Recovery = 88% Analysis Date = 03/05/17 Pct Recovery = 88% Analysis Date = 03/05/17 Pct Recovery = 88% Analysis Date = 02/23/17 Pct Recovery = 88% Analysis Date = 02/23/17 Pct Recovery = 88% Analysis Date = 02/14/17 Pct Recovery = 87% Analysis Date = 02/14/17 Pct Recovery = 87% Analysis Date = 02/04/17 Pct Recovery = 87% Analysis Date = 02/04/17 Pct Recovery = 87% Analysis Date = 01/25/17 Pct Recovery = 87% Analysis Date = 01/25/17 Pct Recovery = 87% Analysis Date = 01/15/17 Pct Recovery = 87% Analysis Date = 01/15/17 Pct Recovery = 87% Analysis Date = 01/05/17 Pct Recovery = 87% Analysis Date = 01/05/17 Pct Recovery = 87% Analysis Date = 12/27/16 Pct Recovery = 87% Analysis Date = 12/27/16 Pct Recovery = 87% Analysis Date = 12/17/16 Pct Recovery = 87% Analysis Date = 12/17/16 Pct Recovery = 87% Analysis Date = 12/07/16 Pct Recovery = 87% Analysis Date = 12/07/16 Pct Recovery = 87% Analysis Date = 11/27/16 Pct Recovery = 87% Analysis Date = 11/27/16 Pct Recovery = 87% Analysis Date = 11/17/16 Pct Recovery = 87% Analysis Date = 11/17/16 Pct Recovery = 87% Analysis Date = 11/08/16 Pct Recovery = 87% Analysis Date = 11/08/16 Pct Recovery = 87% Analysis Date = 10/29/16 Pct Recovery = 87% Analysis Date = 10/29/16 Pct Recovery = 87% Analysis Date = 10/19/16 Pct Recovery = 87% Analysis Date = 10/19/16 Pct Recovery = 87% Analysis Date = 10/09/16 Pct Recovery = 87% Analysis Date = 10/09/16 Pct Recovery = 87% Analysis Date = 09/29/16 Pct Recovery = 87% Analysis Date = 09/29/16 Pct Recovery = 87% Analysis Date = 09/19/16 Pct Recovery = 87% Analysis Date = 09/19/16 Pct Recovery = 87% Analysis Date = 09/10/16 Pct Recovery = 86% Analysis Date = 09/10/16 Pct Recovery = 86% Analysis Date = 08/31/16 Pct Recovery = 86% Analysis Date = 08/31/16 Pct Recovery = 86% Analysis Date = 08/21/16 Pct Recovery = 86% Analysis Date = 08/21/16 Pct Recovery = 86% Analysis Date = 08/11/16 Pct Recovery = 86% Analysis Date = 08/11/16 Pct Recovery = 86% Analysis Date = 08/01/16 Pct Recovery = 86% Analysis Date = 08/01/16 Pct Recovery = 86% Analysis Date = 07/23/16 Pct Recovery = 86% Analysis Date = 07/23/16 Pct Recovery = 86% Analysis Date = 07/13/16 Pct Recovery = 86% Analysis Date = 07/13/16 Pct Recovery = 86% Analysis Date = 07/03/16 Pct Recovery = 86% Analysis Date = 07/03/16 Pct Recovery = 86% Analysis Date = 06/23/16 Pct Recovery = 86% Analysis Date = 06/23/16 Pct Recovery = 86% Analysis Date = 06/13/16 Pct Recovery = 86% Analysis Date = 06/13/16 Pct Recovery = 86% Analysis Date = 06/04/16 Pct Recovery = 85% Analysis Date = 06/04/16 Pct Recovery = 85% Analysis Date = 05/25/16 Pct Recovery = 85% Analysis Date = 05/25/16 Pct Recovery = 85% Analysis Date = 05/15/16 Pct Recovery = 85% Analysis Date = 05/15/16 Pct Recovery = 85% Analysis Date = 05/05/16 Pct Recovery = 85% Analysis Date = 05/05/16 Pct Recovery = 85% Analysis Date = 04/25/16 Pct Recovery = 85% Analysis Date = 04/25/16 Pct Recovery = 85% Analysis Date = 04/16/16 Pct Recovery = 85% Analysis Date = 04/16/16 Pct Recovery = 85% Analysis Date = 04/06/16 Pct Recovery = 85% Analysis Date = 04/06/16 Pct Recovery = 85% Analysis Date = 03/27/16 Pct Recovery = 85% Analysis Date = 03/27/16 Pct Recovery = 85% Analysis Date = 03/17/16 Pct Recovery = 85% Analysis Date = 03/17/16 Pct Recovery = 85% Analysis Date = 03/07/16 Pct Recovery = 84% Analysis Date = 03/07/16 Pct Recovery = 84% Analysis Date = 02/26/16 Pct Recovery = 84% Analysis Date = 02/26/16 Pct Recovery = 84% Analysis Date = 02/17/16 Pct Recovery = 84% Analysis Date = 02/17/16 Pct Recovery = 84% Analysis Date = 02/07/16 Pct Recovery = 84% Analysis Date = 02/07/16 Pct Recovery = 84% Analysis Date = 01/28/16 Pct Recovery = 84% Analysis Date = 01/28/16 Pct Recovery = 84% Analysis Date = 01/18/16 Pct Recovery = 84% Analysis Date = 01/18/16 Pct Recovery = 84% Analysis Date = 01/08/16 Pct Recovery = 84% Analysis Date = 01/08/16 Pct Recovery = 84% Analysis Date = 12/30/15 Pct Recovery = 84% Analysis Date = 12/30/15 Pct Recovery = 84% Analysis Date = 12/20/15 Pct Recovery = 84% Analysis Date = 12/20/15 Pct Recovery = 84% Analysis Date = 12/10/15 Pct Recovery = 84% Analysis Date = 12/10/15 Pct Recovery = 84% Analysis Date = 11/30/15 Pct Recovery = 83% Analysis Date = 11/30/15 Pct Recovery = 83% Analysis Date = 11/20/15 Pct Recovery = 83% Analysis Date = 11/20/15 Pct Recovery = 83% Analysis Date = 11/11/15 Pct Recovery = 83% Analysis Date = 11/11/15 Pct Recovery = 83% Analysis Date = 11/01/15 Pct Recovery = 83% Analysis Date = 11/01/15 Pct Recovery = 83% Analysis Date = 10/22/15 Pct Recovery = 83% Analysis Date = 10/22/15 Pct Recovery = 83% Analysis Date = 10/12/15 Pct Recovery = 83% Analysis Date = 10/12/15 Pct Recovery = 83% Analysis Date = 10/02/15 Pct Recovery = 83% Analysis Date = 10/02/15 Pct Recovery = 83% Analysis Date = 09/23/15 Pct Recovery = 83% Analysis Date = 09/23/15 Pct Recovery = 83% Analysis Date = 09/13/15 Pct Recovery = 83% Analysis Date = 09/13/15 Pct Recovery = 83% Analysis Date = 09/03/15 Pct Recovery = 83% Analysis Date = 09/03/15 Pct Recovery = 83% Analysis Date = 08/24/15 Pct Recovery = 83% Analysis Date = 08/24/15 Pct Recovery = 83% Analysis Date = 08/14/15 Pct Recovery = 82% Analysis Date = 08/14/15 Pct Recovery = 82% Analysis Date = 08/04/15 Pct Recovery = 82% Analysis Date = 08/04/15 Pct Recovery = 82% Analysis Date = 07/26/15 Pct Recovery = 82% Analysis Date = 07/26/15 Pct Recovery = 82% Analysis Date = 07/16/15 Pct Recovery = 82% Analysis Date = 07/16/15 Pct Recovery = 82% Analysis Date = 07/06/15 Pct Recovery = 82% Analysis Date = 07/06/15 Pct Recovery = 82% Analysis Date = 06/26/15 Pct Recovery = 82% Analysis Date = 06/26/15 Pct Recovery = 82% Analysis Date = 06/16/15 Pct Recovery = 82% Analysis Date = 06/16/15 Pct Recovery = 82% Analysis Date = 06/07/15 Pct Recovery = 82% Analysis Date = 06/07/15 Pct Recovery = 82% Analysis Date = 05/28/15 Pct Recovery = 82% Analysis Date = 05/28/15 Pct Recovery = 82% Analysis Date = 05/18/15 Pct Recovery = 82% Analysis Date = 05/18/15 Pct Recovery = 82% Analysis Date = 05/08/15 Pct Recovery = 82% Analysis Date = 05/08/15 Pct Recovery = 82% Analysis Date = 04/28/15 Pct Recovery = 82% Analysis Date = 04/28/15 Pct Recovery = 82% Analysis Date = 04/19/15 Pct Recovery = 82% Analysis Date = 04/19/15 Pct Recovery = 82% Analysis Date = 04/09/15 Pct Recovery = 82% Analysis Date = 04/09/15 Pct Recovery = 82% Analysis Date = 03/30/15 Pct Recovery = 82% Analysis Date = 03/30/15 Pct Recovery = 82% Analysis Date = 03/20/15 Pct Recovery = 82% Analysis Date = 03/20/15 Pct Recovery = 82% Analysis Date = 03/10/15 Pct Recovery = 82% Analysis Date = 03/10/15 Pct Recovery = 82% Analysis Date = 02/28/15 Pct Recovery = 82% Analysis Date = 02/28/15 Pct Recovery = 82% Analysis Date = 02/19/15 Pct Recovery = 82% Analysis Date = 02/19/15 Pct Recovery = 82% Analysis Date = 02/09/15 Pct Recovery = 82% Analysis Date = 02/09/15 Pct Recovery = 82% Analysis Date = 01/30/15 Pct Recovery = 82% Analysis Date = 01/30/15 Pct Recovery = 82% Analysis Date = 01/20/15 Pct Recovery = 82% Analysis Date = 01/20/15 Pct Recovery = 82% Analysis Date = 01/10/15 Pct Recovery = 82% Analysis Date = 01/10/15 Pct Recovery = 82% Analysis Date = 01/01/15 Pct Recovery = 82% Analysis Date = 01/01/15 Pct Recovery = 82% Analysis Date = 12/22/14 Pct Recovery = 82% Analysis Date = 12/22/14 Pct Recovery = 82% Analysis Date = 12/12/14 Pct Recovery = 82% Analysis Date = 12/12/14 Pct Recovery = 82% Analysis Date = 12/02/14 Pct Recovery = 82% Analysis Date = 12/02/14 Pct Recovery = 82% Analysis Date = 11/22/14 Pct Recovery = 82% Analysis Date = 11/22/14 Pct Recovery = 82% Analysis Date = 11/13/14 Pct Recovery = 82% Analysis Date = 11/13/14 Pct Recovery = 82% Analysis Date = 11/03/14 Pct Recovery = 82% Analysis Date = 11/03/14 Pct Recovery = 82% Analysis Date = 10/24/14 Pct Recovery = 82% Analysis Date = 10/24/14 Pct Recovery = 82% Analysis Date = 10/14/14 Pct Recovery = 82% Analysis Date = 10/14/14 Pct Recovery = 82% Analysis Date = 10/04/14 Pct Recovery = 82% Analysis Date = 10/04/14 Pct Recovery = 82% Analysis Date = 09/25/14 Pct Recovery = 82% Analysis Date = 09/25/14 Pct Recovery = 82% Analysis Date = 09/15/14 Pct Recovery = 83% Analysis Date = 09/15/14 Pct Recovery = 83% Analysis Date = 09/05/14 Pct Recovery = 83% Analysis Date = 09/05/14 Pct Recovery = 83% Analysis Date = 08/26/14 Pct Recovery = 83% Analysis Date = 08/26/14 Pct Recovery = 83% Analysis Date = 08/16/14 Pct Recovery = 83% Analysis Date = 08/16/14 Pct Recovery = 83% Analysis Date = 08/06/14 Pct Recovery = 83% Analysis Date = 08/06/14 Pct Recovery = 83% Analysis Date = 07/28/14 Pct Recovery = 83% Analysis Date = 07/28/14 Pct Recovery = 83% Analysis Date = 07/18/14 Pct Recovery = 83% Analysis Date = 07/18/14 Pct Recovery = 83% Analysis Date = 07/08/14 Pct Recovery = 83% Analysis Date = 07/08/14 Pct Recovery = 83% Analysis Date = 06/28/14 Pct Recovery = 84% Analysis Date = 06/28/14 Pct Recovery = 84% Analysis Date = 06/18/14 Pct Recovery = 84% Analysis Date = 06/18/14 Pct Recovery = 84% Analysis Date = 06/09/14 Pct Recovery = 84% Analysis Date = 06/09/14 Pct Recovery = 84% Analysis Date = 05/30/14 Pct Recovery = 84% Analysis Date = 05/30/14 Pct Recovery = 84% Analysis Date = 05/20/14 Pct Recovery = 84% Analysis Date = 05/20/14 Pct Recovery = 84% Analysis Date = 05/10/14 Pct Recovery = 85% Analysis Date = 05/10/14 Pct Recovery = 85% Analysis Date = 04/30/14 Pct Recovery = 85% Analysis Date = 04/30/14 Pct Recovery = 85% Analysis Date = 04/21/14 Pct Recovery = 85% Analysis Date = 04/21/14 Pct Recovery = 85% Analysis Date = 04/11/14 Pct Recovery = 85% Analysis Date = 04/11/14 Pct Recovery = 85% Analysis Date = 04/01/14 Pct Recovery = 85% Analysis Date = 04/01/14 Pct Recovery = 85% Analysis Date = 03/22/14 Pct Recovery = 85% Analysis Date = 03/22/14 Pct Recovery = 85% Analysis Date = 03/12/14 Pct Recovery = 85% Analysis Date = 03/12/14 Pct Recovery = 85% Analysis Date = 03/03/14 Pct Recovery = 86% Analysis Date = 03/03/14 Pct Recovery = 86% Analysis Date = 02/21/14 Pct Recovery = 86% Analysis Date = 02/21/14 Pct Recovery = 86% Analysis Date = 02/11/14 Pct Recovery = 86% Analysis Date = 02/11/14 Pct Recovery = 86% Analysis Date = 02/01/14 Pct Recovery = 86% Analysis Date = 02/01/14 Pct Recovery = 86% Analysis Date = 01/22/14 Pct Recovery = 86% Analysis Date = 01/22/14 Pct Recovery = 86% Analysis Date = 01/12/14 Pct Recovery = 86% Analysis Date = 01/12/14 Pct Recovery = 86% Analysis Date = 01/03/14 Pct Recovery = 87% Analysis Date = 01/03/14 Pct Recovery = 87% Analysis Date = 12/24/13 Pct Recovery = 87% Analysis Date = 12/24/13 Pct Recovery = 87% Analysis Date = 12/14/13 Pct Recovery = 87% Analysis Date = 12/14/13 Pct Recovery = 87% Analysis Date = 12/04/13 Pct Recovery = 87% Analysis Date = 12/04/13 Pct Recovery = 87% Analysis Date = 11/24/13 Pct Recovery = 87% Analysis Date = 11/24/13 Pct Recovery = 87% Analysis Date = 11/15/13 Pct Recovery = 87% Analysis Date = 11/15/13 Pct Recovery = 87% Analysis Date = 11/05/13 Pct Recovery = 87% Analysis Date = 11/05/13 Pct Recovery = 87% Analysis Date = 10/26/13 Pct Recovery = 88% Analysis Date = 10/26/13 Pct Recovery = 88% Analysis Date = 10/16/13 Pct Recovery = 88% Analysis Date = 10/16/13 Pct Recovery = 88% Analysis Date = 10/06/13 Pct Recovery = 88% Analysis Date = 10/06/13 Pct Recovery = 88% Analysis Date = 09/27/13 Pct Recovery = 88% Analysis Date = 09/27/13 Pct Recovery = 88% Analysis Date = 09/17/13 Pct Recovery = 88% Analysis Date = 09/17/13 Pct Recovery = 88% Analysis Date = 09/07/13 Pct Recovery = 88% Analysis Date = 09/07/13 Pct Recovery = 88% Analysis Date = 08/28/13 Pct Recovery = 89% Analysis Date = 08/28/13 Pct Recovery = 89% Analysis Date = 08/18/13 Pct Recovery = 89% Analysis Date = 08/18/13 Pct Recovery = 89% Analysis Date = 08/09/13 Pct Recovery = 89% Analysis Date = 08/09/13 Pct Recovery = 89% Analysis Date = 07/30/13 Pct Recovery = 89% Analysis Date = 07/30/13 Pct Recovery = 89% Analysis Date = 07/20/13 Pct Recovery = 89% Analysis Date = 07/20/13 Pct Recovery = 89% Analysis Date = 07/10/13 Pct Recovery = 89% Analysis Date = 07/10/13 Pct Recovery = 89% Analysis Date = 06/30/13 Pct Recovery = 89% Analysis Date = 06/30/13 Pct Recovery = 89% Analysis Date = 06/20/13 Pct Recovery = 90% Analysis Date = 06/20/13 Pct Recovery = 90% Analysis Date = 06/11/13 Pct Recovery = 90% Analysis Date = 06/11/13 Pct Recovery = 90% Analysis Date = 06/01/13 Pct Recovery = 90% Analysis Date = 06/01/13 Pct Recovery = 90% Analysis Date = 05/22/13 Pct Recovery = 90% Analysis Date = 05/22/13 Pct Recovery = 90% Analysis Date = 05/12/13 Pct Recovery = 90% Analysis Date = 05/12/13 Pct Recovery = 90% Analysis Date = 05/02/13 Pct Recovery = 90% Analysis Date = 05/02/13 Pct Recovery = 90% Analysis Date = 04/23/13 Pct Recovery = 90% Analysis Date = 04/23/13 Pct Recovery = 90% Analysis Date = 04/13/13 Pct Recovery = 91% Analysis Date = 04/13/13 Pct Recovery = 91% Analysis Date = 04/03/13 Pct Recovery = 91% Analysis Date = 04/03/13 Pct Recovery = 91% Analysis Date = 03/24/13 Pct Recovery = 91% Analysis Date = 03/24/13 Pct Recovery = 91% Analysis Date = 03/14/13 Pct Recovery = 91% Analysis Date = 03/14/13 Pct Recovery = 91% Analysis Date = 03/05/13 Pct Recovery = 91% Analysis Date = 03/05/13 Pct Recovery = 91% Analysis Date = 02/23/13 Pct Recovery = 91% Analysis Date = 02/23/13 Pct Recovery = 91% Analysis Date = 02/13/13 Pct Recovery = 92% Analysis Date = 02/13/13 Pct Recovery = 92% Analysis Date = 02/03/13 Pct Recovery = 92% Analysis Date = 02/03/13 Pct Recovery = 92% Analysis Date = 01/24/13 Pct Recovery = 92% Analysis Date = 01/24/13 Pct Recovery = 92% Analysis Date = 01/15/13 Pct Recovery = 92% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
3,5-DICHLOROANILINE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 80 86% 10% 88% 11%
Total 80 86% 10% 88% 11%

Sample Statistics
3,5-DICHLOROANILINE

Characteristic N % % Basis
Plotted 80 95% Spiked
Estimated Values 3 4% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 1 1% Spiked
Spiked 84 .  
False Negatives 3 4% 3 out of 84
Not Spiked 50 .  
False Positives 0 0% 0 out of 50

OBSP Determination:
4-CHLORO-2-METHYLPHENOL
METHOD: 2033 , TESTIDCODE: 61633GCM39

Laboratory ID = 20130250061 Lab Value = 0.097 Expected Conc. = 0.2 Report level label = 0.008 Pct Recovery = 49% Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl SpecificMix = A088380 Laboratory ID = 20140230082 Lab Value = 0.046 Expected Conc. = 0.1 Report level label = 0.008 Pct Recovery = 46% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl SpecificMix = A093651 Laboratory ID = 20140100085 Lab Value = 0.060 Expected Conc. = 0.1 Report level label = 0.008 Pct Recovery = 60% Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl SpecificMix = T1130514013 Laboratory ID = 20132490342 Lab Value = 0.064 Expected Conc. = 0.1 Report level label = 0.008 Pct Recovery = 64% Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl SpecificMix = T1130514013 Laboratory ID = 20132420001 Lab Value = 0.060 Expected Conc. = 0.1 Report level label = 0.008 Pct Recovery = 60% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl SpecificMix = A093651 Laboratory ID = 20130810108 Lab Value = 0.079 Expected Conc. = 0.1 Report level label = 0.008 Pct Recovery = 79% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl SpecificMix = T1120530013 Laboratory ID = 20123560092 Lab Value = 0.066 Expected Conc. = 0.1 Report level label = 0.008 Pct Recovery = 66% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = T1120530013 Laboratory ID = 20172510330 Lab Value = 0.035 Expected Conc. = 0.053 Report level label = 0.008 Pct Recovery = 66% Analysis Date = 12/29/17 SpikeMix = ChemService 6537100: 100 µl & Abs 071817Pest: 100 µl SpecificMix = 071817Pest Laboratory ID = 20131370001 Lab Value = 0.042 Expected Conc. = 0.0505 Report level label = 0.008 Pct Recovery = 83% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl SpecificMix = 1473000 Laboratory ID = 20162860079 Lab Value = 0.037 Expected Conc. = 0.05 Report level label = 0.008 Pct Recovery = 74% Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl SpecificMix = 5054800 Laboratory ID = 20163370001 Lab Value = 0.036 Expected Conc. = 0.05 Report level label = 0.008 Pct Recovery = 71% Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl SpecificMix = LC20138V Laboratory ID = 20161880109 Lab Value = 0.030 Expected Conc. = 0.05 Report level label = 0.008 Pct Recovery = 60% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl SpecificMix = 5054800 Laboratory ID = 20140370077 Lab Value = 0.025 Expected Conc. = 0.05 Report level label = 0.008 Pct Recovery = 50% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl SpecificMix = T1130514013 Laboratory ID = 20132690010 Lab Value = 0.036 Expected Conc. = 0.05 Report level label = 0.008 Pct Recovery = 72% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl SpecificMix = T1130514013 Laboratory ID = 20152750006 Lab Value = 0.024 Expected Conc. = 0.048 Report level label = 0.008 Pct Recovery = 49% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl SpecificMix = EN150514012 Laboratory ID = 20152460215 Lab Value = 0.031 Expected Conc. = 0.048 Report level label = 0.008 Pct Recovery = 65% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl SpecificMix = EN150514012 Laboratory ID = 20171720140 Lab Value = 0.025 Expected Conc. = 0.04 Report level label = 0.008 Pct Recovery = 63% Analysis Date = 08/31/17 SpikeMix = Supelco LC20138V: 80 µl & Phenova B20160331: 80 µl SpecificMix = LC20138V Laboratory ID = 20171380001 Lab Value = 0.020 Expected Conc. = 0.04 Report level label = 0.008 Pct Recovery = 51% Analysis Date = 06/07/17 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 5054800 Laboratory ID = 20170960001 Lab Value = 0.024 Expected Conc. = 0.04 Report level label = 0.008 Pct Recovery = 61% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl SpecificMix = 5054800 Laboratory ID = 20170740063 Lab Value = 0.013 Expected Conc. = 0.04 Report level label = 0.008 Pct Recovery = 32% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl SpecificMix = LC20138V Laboratory ID = 20161740258 Lab Value = 0.015 Expected Conc. = 0.04 Report level label = 0.008 Pct Recovery = 39% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 5054800 Laboratory ID = 20161470001 Lab Value = 0.023 Expected Conc. = 0.04 Report level label = 0.008 Pct Recovery = 58% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl SpecificMix = LC20138V Laboratory ID = 20140860102 Lab Value = 0.024 Expected Conc. = 0.04 Report level label = 0.008 Pct Recovery = 61% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl SpecificMix = A093651 Laboratory ID = 20133400002 Lab Value = 0.028 Expected Conc. = 0.04 Report level label = 0.008 Pct Recovery = 70% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = A093651 Laboratory ID = 20132910008 Lab Value = 0.024 Expected Conc. = 0.04 Report level label = 0.008 Pct Recovery = 61% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = A093651 Laboratory ID = 20131920149 Lab Value = 0.028 Expected Conc. = 0.04 Report level label = 0.008 Pct Recovery = 69% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl SpecificMix = A093651 Laboratory ID = 20131230084 Lab Value = 0.031 Expected Conc. = 0.04 Report level label = 0.008 Pct Recovery = 78% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl SpecificMix = A088380 Laboratory ID = 20130650005 Lab Value = 0.026 Expected Conc. = 0.04 Report level label = 0.008 Pct Recovery = 65% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl SpecificMix = A088380 Laboratory ID = 20130390105 Lab Value = 0.027 Expected Conc. = 0.04 Report level label = 0.008 Pct Recovery = 66% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl SpecificMix = T1120530013 Laboratory ID = 20150720069 Lab Value = 0.011 Expected Conc. = 0.0318 Report level label = 0.008 Pct Recovery = 34% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 03DD006 Laboratory ID = 20143110108 Lab Value = 0.016 Expected Conc. = 0.0318 Report level label = 0.008 Pct Recovery = 51% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 03DD006 Laboratory ID = 20142960086 Lab Value = 0.018 Expected Conc. = 0.0318 Report level label = 0.008 Pct Recovery = 55% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 03DD006 Laboratory ID = 20142720002 Lab Value = 0.014 Expected Conc. = 0.0318 Report level label = 0.008 Pct Recovery = 45% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl SpecificMix = LC06435 Laboratory ID = 20142530087 Lab Value = 0.018 Expected Conc. = 0.0318 Report level label = 0.008 Pct Recovery = 55% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl SpecificMix = LC06435 Laboratory ID = 20142270001 Lab Value = 0.019 Expected Conc. = 0.0318 Report level label = 0.008 Pct Recovery = 58% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl SpecificMix = 03DD006 Laboratory ID = 20141570088 Lab Value = 0.024 Expected Conc. = 0.0318 Report level label = 0.008 Pct Recovery = 75% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl SpecificMix = LC06435 Laboratory ID = 20141220025 Lab Value = 0.026 Expected Conc. = 0.0318 Report level label = 0.008 Pct Recovery = 83% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl SpecificMix = LC06435 Laboratory ID = 20172560101 Lab Value = 0.015 Expected Conc. = 0.025 Report level label = 0.008 Pct Recovery = 60% Analysis Date = 12/22/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6567600: 50 µl SpecificMix = 6567600 Laboratory ID = 20160630046 Lab Value = 0.012 Expected Conc. = 0.024 Report level label = 0.008 Pct Recovery = 50% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = EN150514012 Laboratory ID = 20153440001 Lab Value = 0.011 Expected Conc. = 0.024 Report level label = 0.008 Pct Recovery = 45% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = EN150514012 Laboratory ID = 20152330039 Lab Value = 0.016 Expected Conc. = 0.024 Report level label = 0.008 Pct Recovery = 66% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl SpecificMix = 041415 Laboratory ID = 20151900132 Lab Value = 0.017 Expected Conc. = 0.024 Report level label = 0.008 Pct Recovery = 73% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl SpecificMix = 041415 Laboratory ID = 20151270112 Lab Value = 0.014 Expected Conc. = 0.024 Report level label = 0.008 Pct Recovery = 58% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl SpecificMix = 041415 Laboratory ID = 20140730138 Lab Value = 0.009 Expected Conc. = 0.0202 Report level label = 0.008 Pct Recovery = 43% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 1473000 Laboratory ID = 20133470008 Lab Value = 0.017 Expected Conc. = 0.0202 Report level label = 0.008 Pct Recovery = 83% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl SpecificMix = 1473000 Laboratory ID = 20133310030 Lab Value = 0.015 Expected Conc. = 0.0202 Report level label = 0.008 Pct Recovery = 76% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl SpecificMix = 1473000 Laboratory ID = 20131790009 Lab Value = 0.013 Expected Conc. = 0.0202 Report level label = 0.008 Pct Recovery = 66% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl SpecificMix = 1473000 Laboratory ID = 20131650073 Lab Value = 0.014 Expected Conc. = 0.0202 Report level label = 0.008 Pct Recovery = 69% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl SpecificMix = 1473000 Laboratory ID = 20171940002 Lab Value = 0.015 Expected Conc. = 0.02 Report level label = 0.008 Pct Recovery = 76% Analysis Date = 11/10/17 SpikeMix = ChemService 5054800: 40 µl & NSI 041816: 40 µl SpecificMix = 5054800 Laboratory ID = 20171510080 Lab Value = 0.014 Expected Conc. = 0.02 Report level label = 0.008 Pct Recovery = 70% Analysis Date = 06/09/17 SpikeMix = Supelco LC20138V: 40 µl & Crescent 03FF076: 40 µl SpecificMix = LC20138V Laboratory ID = 20170460061 Lab Value = 0.011 Expected Conc. = 0.02 Report level label = 0.008 Pct Recovery = 57% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl SpecificMix = 5054800 Laboratory ID = 20162520001 Lab Value = 0.015 Expected Conc. = 0.02 Report level label = 0.008 Pct Recovery = 77% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl SpecificMix = LC20138V Laboratory ID = 20163560019 Lab Value = 0.012 Expected Conc. = 0.02 Report level label = 0.008 Pct Recovery = 58% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl SpecificMix = 5054800 Laboratory ID = 20162660005 Lab Value = 0.012 Expected Conc. = 0.02 Report level label = 0.008 Pct Recovery = 59% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl SpecificMix = LC20138V Laboratory ID = 20162150213 Lab Value = 0.011 Expected Conc. = 0.02 Report level label = 0.008 Pct Recovery = 56% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl SpecificMix = 5054800 Laboratory ID = 20162020124 Lab Value = 0.013 Expected Conc. = 0.02 Report level label = 0.008 Pct Recovery = 66% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl SpecificMix = LC20138V Laboratory ID = 20133050050 Lab Value = 0.016 Expected Conc. = 0.02 Report level label = 0.008 Pct Recovery = 82% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl SpecificMix = T1130514013 Laboratory ID = 20132280016 Lab Value = 0.018 Expected Conc. = 0.02 Report level label = 0.008 Pct Recovery = 90% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl SpecificMix = T1130514013 Laboratory ID = 20172780018 Lab Value = 0.010 Expected Conc. = 0.0159 Report level label = 0.008 Pct Recovery = 64% Analysis Date = 02/08/18 SpikeMix = ChemService 6537100: 30 µl & Abs 071817Pest: 30 µl SpecificMix = 071817Pest Laboratory ID = 20150150115 Lab Value = 0.010 Expected Conc. = 0.0159 Report level label = 0.008 Pct Recovery = 62% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl SpecificMix = LC06435 Laboratory ID = 20143370094 Lab Value = 0.008 Expected Conc. = 0.0159 Report level label = 0.008 Pct Recovery = 52% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl SpecificMix = LC06435 Laboratory ID = 20142200164 Lab Value = 0.011 Expected Conc. = 0.0159 Report level label = 0.008 Pct Recovery = 68% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 03DD006 Laboratory ID = 20141910243 Lab Value = 0.009 Expected Conc. = 0.0159 Report level label = 0.008 Pct Recovery = 55% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = LC06435 Laboratory ID = 20141840097 Lab Value = 0.009 Expected Conc. = 0.0159 Report level label = 0.008 Pct Recovery = 55% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl SpecificMix = LC06435 Laboratory ID = 20141640076 Lab Value = 0.011 Expected Conc. = 0.0159 Report level label = 0.008 Pct Recovery = 68% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = 03DD006 Laboratory ID = 20141420140 Lab Value = 0.009 Expected Conc. = 0.0159 Report level label = 0.008 Pct Recovery = 56% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 03DD006 Laboratory ID = 20141080004 Lab Value = 0.012 Expected Conc. = 0.0159 Report level label = 0.008 Pct Recovery = 74% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl SpecificMix = 03DD006 Laboratory ID = 20161050143 Lab Value = 0.008 Expected Conc. = 0.012 Report level label = 0.008 Pct Recovery = 69% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 041415 Laboratory ID = 20160560044 Lab Value = 0.007 Expected Conc. = 0.012 Report level label = 0.008 Pct Recovery = 54% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl SpecificMix = 041415 Laboratory ID = 20160210080 Lab Value = 0.007 Expected Conc. = 0.012 Report level label = 0.008 Pct Recovery = 55% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 041415 Laboratory ID = 20160070059 Lab Value = 0.006 Expected Conc. = 0.012 Report level label = 0.008 Pct Recovery = 46% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = EN150514012 Laboratory ID = 20153160001 Lab Value = 0.008 Expected Conc. = 0.012 Report level label = 0.008 Pct Recovery = 67% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = EN150514012 Laboratory ID = 20152950078 Lab Value = 0.005 Expected Conc. = 0.012 Report level label = 0.008 Pct Recovery = 45% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 041415 Laboratory ID = 20152040177 Lab Value = 0.007 Expected Conc. = 0.012 Report level label = 0.008 Pct Recovery = 62% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl SpecificMix = 041415 Laboratory ID = 20151760208 Lab Value = 0.007 Expected Conc. = 0.012 Report level label = 0.008 Pct Recovery = 56% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl SpecificMix = EN150514012 Laboratory ID = 20151480170 Lab Value = 0.008 Expected Conc. = 0.012 Report level label = 0.008 Pct Recovery = 68% Analysis Date = 06/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150514012 Laboratory ID = 20151210037 Lab Value = 0.008 Expected Conc. = 0.012 Report level label = 0.008 Pct Recovery = 70% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 041415 Analysis Date = 02/08/18 Pct Recovery = 64% Analysis Date = 01/29/18 Pct Recovery = 64% Analysis Date = 01/29/18 Pct Recovery = 64% Analysis Date = 01/20/18 Pct Recovery = 64% Analysis Date = 01/20/18 Pct Recovery = 64% Analysis Date = 01/11/18 Pct Recovery = 64% Analysis Date = 01/11/18 Pct Recovery = 64% Analysis Date = 01/02/18 Pct Recovery = 64% Analysis Date = 01/02/18 Pct Recovery = 64% Analysis Date = 12/23/17 Pct Recovery = 64% Analysis Date = 12/23/17 Pct Recovery = 64% Analysis Date = 12/14/17 Pct Recovery = 64% Analysis Date = 12/14/17 Pct Recovery = 64% Analysis Date = 12/05/17 Pct Recovery = 64% Analysis Date = 12/05/17 Pct Recovery = 64% Analysis Date = 11/26/17 Pct Recovery = 63% Analysis Date = 11/26/17 Pct Recovery = 63% Analysis Date = 11/16/17 Pct Recovery = 63% Analysis Date = 11/16/17 Pct Recovery = 63% Analysis Date = 11/07/17 Pct Recovery = 63% Analysis Date = 11/07/17 Pct Recovery = 63% Analysis Date = 10/29/17 Pct Recovery = 63% Analysis Date = 10/29/17 Pct Recovery = 63% Analysis Date = 10/20/17 Pct Recovery = 63% Analysis Date = 10/20/17 Pct Recovery = 63% Analysis Date = 10/10/17 Pct Recovery = 63% Analysis Date = 10/10/17 Pct Recovery = 63% Analysis Date = 10/01/17 Pct Recovery = 63% Analysis Date = 10/01/17 Pct Recovery = 63% Analysis Date = 09/22/17 Pct Recovery = 63% Analysis Date = 09/22/17 Pct Recovery = 63% Analysis Date = 09/13/17 Pct Recovery = 63% Analysis Date = 09/13/17 Pct Recovery = 63% Analysis Date = 09/03/17 Pct Recovery = 63% Analysis Date = 09/03/17 Pct Recovery = 63% Analysis Date = 08/25/17 Pct Recovery = 62% Analysis Date = 08/25/17 Pct Recovery = 62% Analysis Date = 08/16/17 Pct Recovery = 62% Analysis Date = 08/16/17 Pct Recovery = 62% Analysis Date = 08/07/17 Pct Recovery = 62% Analysis Date = 08/07/17 Pct Recovery = 62% Analysis Date = 07/28/17 Pct Recovery = 62% Analysis Date = 07/28/17 Pct Recovery = 62% Analysis Date = 07/19/17 Pct Recovery = 62% Analysis Date = 07/19/17 Pct Recovery = 62% Analysis Date = 07/10/17 Pct Recovery = 62% Analysis Date = 07/10/17 Pct Recovery = 62% Analysis Date = 07/01/17 Pct Recovery = 62% Analysis Date = 07/01/17 Pct Recovery = 62% Analysis Date = 06/21/17 Pct Recovery = 62% Analysis Date = 06/21/17 Pct Recovery = 62% Analysis Date = 06/12/17 Pct Recovery = 62% Analysis Date = 06/12/17 Pct Recovery = 62% Analysis Date = 06/03/17 Pct Recovery = 61% Analysis Date = 06/03/17 Pct Recovery = 61% Analysis Date = 05/25/17 Pct Recovery = 61% Analysis Date = 05/25/17 Pct Recovery = 61% Analysis Date = 05/15/17 Pct Recovery = 61% Analysis Date = 05/15/17 Pct Recovery = 61% Analysis Date = 05/06/17 Pct Recovery = 61% Analysis Date = 05/06/17 Pct Recovery = 61% Analysis Date = 04/27/17 Pct Recovery = 61% Analysis Date = 04/27/17 Pct Recovery = 61% Analysis Date = 04/18/17 Pct Recovery = 61% Analysis Date = 04/18/17 Pct Recovery = 61% Analysis Date = 04/08/17 Pct Recovery = 61% Analysis Date = 04/08/17 Pct Recovery = 61% Analysis Date = 03/30/17 Pct Recovery = 61% Analysis Date = 03/30/17 Pct Recovery = 61% Analysis Date = 03/21/17 Pct Recovery = 61% Analysis Date = 03/21/17 Pct Recovery = 61% Analysis Date = 03/12/17 Pct Recovery = 61% Analysis Date = 03/12/17 Pct Recovery = 61% Analysis Date = 03/02/17 Pct Recovery = 60% Analysis Date = 03/02/17 Pct Recovery = 60% Analysis Date = 02/21/17 Pct Recovery = 60% Analysis Date = 02/21/17 Pct Recovery = 60% Analysis Date = 02/12/17 Pct Recovery = 60% Analysis Date = 02/12/17 Pct Recovery = 60% Analysis Date = 02/03/17 Pct Recovery = 60% Analysis Date = 02/03/17 Pct Recovery = 60% Analysis Date = 01/24/17 Pct Recovery = 60% Analysis Date = 01/24/17 Pct Recovery = 60% Analysis Date = 01/15/17 Pct Recovery = 60% Analysis Date = 01/15/17 Pct Recovery = 60% Analysis Date = 01/06/17 Pct Recovery = 60% Analysis Date = 01/06/17 Pct Recovery = 60% Analysis Date = 12/28/16 Pct Recovery = 60% Analysis Date = 12/28/16 Pct Recovery = 60% Analysis Date = 12/18/16 Pct Recovery = 60% Analysis Date = 12/18/16 Pct Recovery = 60% Analysis Date = 12/09/16 Pct Recovery = 60% Analysis Date = 12/09/16 Pct Recovery = 60% Analysis Date = 11/30/16 Pct Recovery = 60% Analysis Date = 11/30/16 Pct Recovery = 60% Analysis Date = 11/21/16 Pct Recovery = 59% Analysis Date = 11/21/16 Pct Recovery = 59% Analysis Date = 11/11/16 Pct Recovery = 59% Analysis Date = 11/11/16 Pct Recovery = 59% Analysis Date = 11/02/16 Pct Recovery = 59% Analysis Date = 11/02/16 Pct Recovery = 59% Analysis Date = 10/24/16 Pct Recovery = 59% Analysis Date = 10/24/16 Pct Recovery = 59% Analysis Date = 10/15/16 Pct Recovery = 59% Analysis Date = 10/15/16 Pct Recovery = 59% Analysis Date = 10/05/16 Pct Recovery = 59% Analysis Date = 10/05/16 Pct Recovery = 59% Analysis Date = 09/26/16 Pct Recovery = 59% Analysis Date = 09/26/16 Pct Recovery = 59% Analysis Date = 09/17/16 Pct Recovery = 59% Analysis Date = 09/17/16 Pct Recovery = 59% Analysis Date = 09/08/16 Pct Recovery = 59% Analysis Date = 09/08/16 Pct Recovery = 59% Analysis Date = 08/29/16 Pct Recovery = 59% Analysis Date = 08/29/16 Pct Recovery = 59% Analysis Date = 08/20/16 Pct Recovery = 59% Analysis Date = 08/20/16 Pct Recovery = 59% Analysis Date = 08/11/16 Pct Recovery = 59% Analysis Date = 08/11/16 Pct Recovery = 59% Analysis Date = 08/02/16 Pct Recovery = 59% Analysis Date = 08/02/16 Pct Recovery = 59% Analysis Date = 07/23/16 Pct Recovery = 58% Analysis Date = 07/23/16 Pct Recovery = 58% Analysis Date = 07/14/16 Pct Recovery = 58% Analysis Date = 07/14/16 Pct Recovery = 58% Analysis Date = 07/05/16 Pct Recovery = 58% Analysis Date = 07/05/16 Pct Recovery = 58% Analysis Date = 06/26/16 Pct Recovery = 58% Analysis Date = 06/26/16 Pct Recovery = 58% Analysis Date = 06/16/16 Pct Recovery = 58% Analysis Date = 06/16/16 Pct Recovery = 58% Analysis Date = 06/07/16 Pct Recovery = 58% Analysis Date = 06/07/16 Pct Recovery = 58% Analysis Date = 05/29/16 Pct Recovery = 58% Analysis Date = 05/29/16 Pct Recovery = 58% Analysis Date = 05/20/16 Pct Recovery = 58% Analysis Date = 05/20/16 Pct Recovery = 58% Analysis Date = 05/10/16 Pct Recovery = 58% Analysis Date = 05/10/16 Pct Recovery = 58% Analysis Date = 05/01/16 Pct Recovery = 58% Analysis Date = 05/01/16 Pct Recovery = 58% Analysis Date = 04/22/16 Pct Recovery = 58% Analysis Date = 04/22/16 Pct Recovery = 58% Analysis Date = 04/13/16 Pct Recovery = 58% Analysis Date = 04/13/16 Pct Recovery = 58% Analysis Date = 04/03/16 Pct Recovery = 58% Analysis Date = 04/03/16 Pct Recovery = 58% Analysis Date = 03/25/16 Pct Recovery = 58% Analysis Date = 03/25/16 Pct Recovery = 58% Analysis Date = 03/16/16 Pct Recovery = 58% Analysis Date = 03/16/16 Pct Recovery = 58% Analysis Date = 03/07/16 Pct Recovery = 58% Analysis Date = 03/07/16 Pct Recovery = 58% Analysis Date = 02/26/16 Pct Recovery = 58% Analysis Date = 02/26/16 Pct Recovery = 58% Analysis Date = 02/17/16 Pct Recovery = 58% Analysis Date = 02/17/16 Pct Recovery = 58% Analysis Date = 02/08/16 Pct Recovery = 57% Analysis Date = 02/08/16 Pct Recovery = 57% Analysis Date = 01/30/16 Pct Recovery = 57% Analysis Date = 01/30/16 Pct Recovery = 57% Analysis Date = 01/20/16 Pct Recovery = 57% Analysis Date = 01/20/16 Pct Recovery = 57% Analysis Date = 01/11/16 Pct Recovery = 57% Analysis Date = 01/11/16 Pct Recovery = 57% Analysis Date = 01/02/16 Pct Recovery = 57% Analysis Date = 01/02/16 Pct Recovery = 57% Analysis Date = 12/24/15 Pct Recovery = 57% Analysis Date = 12/24/15 Pct Recovery = 57% Analysis Date = 12/14/15 Pct Recovery = 57% Analysis Date = 12/14/15 Pct Recovery = 57% Analysis Date = 12/05/15 Pct Recovery = 57% Analysis Date = 12/05/15 Pct Recovery = 57% Analysis Date = 11/26/15 Pct Recovery = 57% Analysis Date = 11/26/15 Pct Recovery = 57% Analysis Date = 11/17/15 Pct Recovery = 57% Analysis Date = 11/17/15 Pct Recovery = 57% Analysis Date = 11/07/15 Pct Recovery = 57% Analysis Date = 11/07/15 Pct Recovery = 57% Analysis Date = 10/29/15 Pct Recovery = 57% Analysis Date = 10/29/15 Pct Recovery = 57% Analysis Date = 10/20/15 Pct Recovery = 57% Analysis Date = 10/20/15 Pct Recovery = 57% Analysis Date = 10/11/15 Pct Recovery = 57% Analysis Date = 10/11/15 Pct Recovery = 57% Analysis Date = 10/01/15 Pct Recovery = 57% Analysis Date = 10/01/15 Pct Recovery = 57% Analysis Date = 09/22/15 Pct Recovery = 57% Analysis Date = 09/22/15 Pct Recovery = 57% Analysis Date = 09/13/15 Pct Recovery = 57% Analysis Date = 09/13/15 Pct Recovery = 57% Analysis Date = 09/04/15 Pct Recovery = 57% Analysis Date = 09/04/15 Pct Recovery = 57% Analysis Date = 08/25/15 Pct Recovery = 57% Analysis Date = 08/25/15 Pct Recovery = 57% Analysis Date = 08/16/15 Pct Recovery = 57% Analysis Date = 08/16/15 Pct Recovery = 57% Analysis Date = 08/07/15 Pct Recovery = 57% Analysis Date = 08/07/15 Pct Recovery = 57% Analysis Date = 07/29/15 Pct Recovery = 57% Analysis Date = 07/29/15 Pct Recovery = 57% Analysis Date = 07/19/15 Pct Recovery = 57% Analysis Date = 07/19/15 Pct Recovery = 57% Analysis Date = 07/10/15 Pct Recovery = 57% Analysis Date = 07/10/15 Pct Recovery = 57% Analysis Date = 07/01/15 Pct Recovery = 57% Analysis Date = 07/01/15 Pct Recovery = 57% Analysis Date = 06/22/15 Pct Recovery = 58% Analysis Date = 06/22/15 Pct Recovery = 58% Analysis Date = 06/12/15 Pct Recovery = 58% Analysis Date = 06/12/15 Pct Recovery = 58% Analysis Date = 06/03/15 Pct Recovery = 58% Analysis Date = 06/03/15 Pct Recovery = 58% Analysis Date = 05/25/15 Pct Recovery = 58% Analysis Date = 05/25/15 Pct Recovery = 58% Analysis Date = 05/16/15 Pct Recovery = 58% Analysis Date = 05/16/15 Pct Recovery = 58% Analysis Date = 05/06/15 Pct Recovery = 58% Analysis Date = 05/06/15 Pct Recovery = 58% Analysis Date = 04/27/15 Pct Recovery = 58% Analysis Date = 04/27/15 Pct Recovery = 58% Analysis Date = 04/18/15 Pct Recovery = 58% Analysis Date = 04/18/15 Pct Recovery = 58% Analysis Date = 04/09/15 Pct Recovery = 58% Analysis Date = 04/09/15 Pct Recovery = 58% Analysis Date = 03/30/15 Pct Recovery = 58% Analysis Date = 03/30/15 Pct Recovery = 58% Analysis Date = 03/21/15 Pct Recovery = 59% Analysis Date = 03/21/15 Pct Recovery = 59% Analysis Date = 03/12/15 Pct Recovery = 59% Analysis Date = 03/12/15 Pct Recovery = 59% Analysis Date = 03/03/15 Pct Recovery = 59% Analysis Date = 03/03/15 Pct Recovery = 59% Analysis Date = 02/21/15 Pct Recovery = 59% Analysis Date = 02/21/15 Pct Recovery = 59% Analysis Date = 02/12/15 Pct Recovery = 59% Analysis Date = 02/12/15 Pct Recovery = 59% Analysis Date = 02/03/15 Pct Recovery = 59% Analysis Date = 02/03/15 Pct Recovery = 59% Analysis Date = 01/25/15 Pct Recovery = 59% Analysis Date = 01/25/15 Pct Recovery = 59% Analysis Date = 01/15/15 Pct Recovery = 59% Analysis Date = 01/15/15 Pct Recovery = 59% Analysis Date = 01/06/15 Pct Recovery = 59% Analysis Date = 01/06/15 Pct Recovery = 59% Analysis Date = 12/28/14 Pct Recovery = 59% Analysis Date = 12/28/14 Pct Recovery = 59% Analysis Date = 12/19/14 Pct Recovery = 60% Analysis Date = 12/19/14 Pct Recovery = 60% Analysis Date = 12/09/14 Pct Recovery = 60% Analysis Date = 12/09/14 Pct Recovery = 60% Analysis Date = 11/30/14 Pct Recovery = 60% Analysis Date = 11/30/14 Pct Recovery = 60% Analysis Date = 11/21/14 Pct Recovery = 60% Analysis Date = 11/21/14 Pct Recovery = 60% Analysis Date = 11/12/14 Pct Recovery = 60% Analysis Date = 11/12/14 Pct Recovery = 60% Analysis Date = 11/02/14 Pct Recovery = 60% Analysis Date = 11/02/14 Pct Recovery = 60% Analysis Date = 10/24/14 Pct Recovery = 60% Analysis Date = 10/24/14 Pct Recovery = 60% Analysis Date = 10/15/14 Pct Recovery = 60% Analysis Date = 10/15/14 Pct Recovery = 60% Analysis Date = 10/06/14 Pct Recovery = 60% Analysis Date = 10/06/14 Pct Recovery = 60% Analysis Date = 09/26/14 Pct Recovery = 60% Analysis Date = 09/26/14 Pct Recovery = 60% Analysis Date = 09/17/14 Pct Recovery = 60% Analysis Date = 09/17/14 Pct Recovery = 60% Analysis Date = 09/08/14 Pct Recovery = 61% Analysis Date = 09/08/14 Pct Recovery = 61% Analysis Date = 08/30/14 Pct Recovery = 61% Analysis Date = 08/30/14 Pct Recovery = 61% Analysis Date = 08/20/14 Pct Recovery = 61% Analysis Date = 08/20/14 Pct Recovery = 61% Analysis Date = 08/11/14 Pct Recovery = 61% Analysis Date = 08/11/14 Pct Recovery = 61% Analysis Date = 08/02/14 Pct Recovery = 61% Analysis Date = 08/02/14 Pct Recovery = 61% Analysis Date = 07/24/14 Pct Recovery = 61% Analysis Date = 07/24/14 Pct Recovery = 61% Analysis Date = 07/14/14 Pct Recovery = 61% Analysis Date = 07/14/14 Pct Recovery = 61% Analysis Date = 07/05/14 Pct Recovery = 61% Analysis Date = 07/05/14 Pct Recovery = 61% Analysis Date = 06/26/14 Pct Recovery = 61% Analysis Date = 06/26/14 Pct Recovery = 61% Analysis Date = 06/17/14 Pct Recovery = 62% Analysis Date = 06/17/14 Pct Recovery = 62% Analysis Date = 06/07/14 Pct Recovery = 62% Analysis Date = 06/07/14 Pct Recovery = 62% Analysis Date = 05/29/14 Pct Recovery = 62% Analysis Date = 05/29/14 Pct Recovery = 62% Analysis Date = 05/20/14 Pct Recovery = 62% Analysis Date = 05/20/14 Pct Recovery = 62% Analysis Date = 05/11/14 Pct Recovery = 62% Analysis Date = 05/11/14 Pct Recovery = 62% Analysis Date = 05/01/14 Pct Recovery = 63% Analysis Date = 05/01/14 Pct Recovery = 63% Analysis Date = 04/22/14 Pct Recovery = 63% Analysis Date = 04/22/14 Pct Recovery = 63% Analysis Date = 04/13/14 Pct Recovery = 63% Analysis Date = 04/13/14 Pct Recovery = 63% Analysis Date = 04/04/14 Pct Recovery = 63% Analysis Date = 04/04/14 Pct Recovery = 63% Analysis Date = 03/25/14 Pct Recovery = 63% Analysis Date = 03/25/14 Pct Recovery = 63% Analysis Date = 03/16/14 Pct Recovery = 64% Analysis Date = 03/16/14 Pct Recovery = 64% Analysis Date = 03/07/14 Pct Recovery = 64% Analysis Date = 03/07/14 Pct Recovery = 64% Analysis Date = 02/26/14 Pct Recovery = 64% Analysis Date = 02/26/14 Pct Recovery = 64% Analysis Date = 02/16/14 Pct Recovery = 64% Analysis Date = 02/16/14 Pct Recovery = 64% Analysis Date = 02/07/14 Pct Recovery = 65% Analysis Date = 02/07/14 Pct Recovery = 65% Analysis Date = 01/29/14 Pct Recovery = 65% Analysis Date = 01/29/14 Pct Recovery = 65% Analysis Date = 01/20/14 Pct Recovery = 65% Analysis Date = 01/20/14 Pct Recovery = 65% Analysis Date = 01/10/14 Pct Recovery = 65% Analysis Date = 01/10/14 Pct Recovery = 65% Analysis Date = 01/01/14 Pct Recovery = 66% Analysis Date = 01/01/14 Pct Recovery = 66% Analysis Date = 12/23/13 Pct Recovery = 66% Analysis Date = 12/23/13 Pct Recovery = 66% Analysis Date = 12/14/13 Pct Recovery = 66% Analysis Date = 12/14/13 Pct Recovery = 66% Analysis Date = 12/04/13 Pct Recovery = 66% Analysis Date = 12/04/13 Pct Recovery = 66% Analysis Date = 11/25/13 Pct Recovery = 66% Analysis Date = 11/25/13 Pct Recovery = 66% Analysis Date = 11/16/13 Pct Recovery = 66% Analysis Date = 11/16/13 Pct Recovery = 66% Analysis Date = 11/07/13 Pct Recovery = 67% Analysis Date = 11/07/13 Pct Recovery = 67% Analysis Date = 10/28/13 Pct Recovery = 67% Analysis Date = 10/28/13 Pct Recovery = 67% Analysis Date = 10/19/13 Pct Recovery = 67% Analysis Date = 10/19/13 Pct Recovery = 67% Analysis Date = 10/10/13 Pct Recovery = 67% Analysis Date = 10/10/13 Pct Recovery = 67% Analysis Date = 10/01/13 Pct Recovery = 67% Analysis Date = 10/01/13 Pct Recovery = 67% Analysis Date = 09/21/13 Pct Recovery = 67% Analysis Date = 09/21/13 Pct Recovery = 67% Analysis Date = 09/12/13 Pct Recovery = 68% Analysis Date = 09/12/13 Pct Recovery = 68% Analysis Date = 09/03/13 Pct Recovery = 68% Analysis Date = 09/03/13 Pct Recovery = 68% Analysis Date = 08/25/13 Pct Recovery = 68% Analysis Date = 08/25/13 Pct Recovery = 68% Analysis Date = 08/15/13 Pct Recovery = 68% Analysis Date = 08/15/13 Pct Recovery = 68% Analysis Date = 08/06/13 Pct Recovery = 68% Analysis Date = 08/06/13 Pct Recovery = 68% Analysis Date = 07/28/13 Pct Recovery = 68% Analysis Date = 07/28/13 Pct Recovery = 68% Analysis Date = 07/19/13 Pct Recovery = 69% Analysis Date = 07/19/13 Pct Recovery = 69% Analysis Date = 07/09/13 Pct Recovery = 69% Analysis Date = 07/09/13 Pct Recovery = 69% Analysis Date = 06/30/13 Pct Recovery = 69% Analysis Date = 06/30/13 Pct Recovery = 69% Analysis Date = 06/21/13 Pct Recovery = 69% Analysis Date = 06/21/13 Pct Recovery = 69% Analysis Date = 06/12/13 Pct Recovery = 69% Analysis Date = 06/12/13 Pct Recovery = 69% Analysis Date = 06/02/13 Pct Recovery = 69% Analysis Date = 06/02/13 Pct Recovery = 69% Analysis Date = 05/24/13 Pct Recovery = 70% Analysis Date = 05/24/13 Pct Recovery = 70% Analysis Date = 05/15/13 Pct Recovery = 70% Analysis Date = 05/15/13 Pct Recovery = 70% Analysis Date = 05/06/13 Pct Recovery = 70% Analysis Date = 05/06/13 Pct Recovery = 70% Analysis Date = 04/26/13 Pct Recovery = 70% Analysis Date = 04/26/13 Pct Recovery = 70% Analysis Date = 04/17/13 Pct Recovery = 70% Analysis Date = 04/17/13 Pct Recovery = 70% Analysis Date = 04/08/13 Pct Recovery = 70% Analysis Date = 04/08/13 Pct Recovery = 70% Analysis Date = 03/30/13 Pct Recovery = 71% Analysis Date = 03/30/13 Pct Recovery = 71% Analysis Date = 03/20/13 Pct Recovery = 71% Analysis Date = 03/20/13 Pct Recovery = 71% Analysis Date = 03/11/13 Pct Recovery = 71% Analysis Date = 03/11/13 Pct Recovery = 71% Analysis Date = 03/02/13 Pct Recovery = 71% Analysis Date = 03/02/13 Pct Recovery = 71% Analysis Date = 02/21/13 Pct Recovery = 71% Analysis Date = 02/21/13 Pct Recovery = 71% Analysis Date = 02/11/13 Pct Recovery = 71% Analysis Date = 02/11/13 Pct Recovery = 71% Analysis Date = 02/02/13 Pct Recovery = 71% Analysis Date = 02/02/13 Pct Recovery = 71% Analysis Date = 01/24/13 Pct Recovery = 72% Analysis Date = 01/24/13 Pct Recovery = 72% Analysis Date = 01/15/13 Pct Recovery = 72% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
4-CHLORO-2-METHYLPHENOL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 77 62% 12% 62% 11%
Total 77 62% 12% 62% 11%

Sample Statistics
4-CHLORO-2-METHYLPHENOL

Characteristic N % % Basis
Plotted 77 100% Spiked
Estimated Values 77 100% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 77 .  
False Negatives 0 0% 0 out of 77
Not Spiked 41 .  
False Positives 0 0% 0 out of 41

OBSP Determination:
ACETOCHLOR
METHOD: 2033 , TESTIDCODE: 49260GCM33

Laboratory ID = 20130250061 Lab Value = 0.231 Expected Conc. = 0.3 Report level label = 0.01 Pct Recovery = 77% Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl SpecificMix = A088380 Laboratory ID = 20140100085 Lab Value = 0.221 Expected Conc. = 0.25 Report level label = 0.01 Pct Recovery = 88% Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl SpecificMix = T1130514013 Laboratory ID = 20132490342 Lab Value = 0.239 Expected Conc. = 0.25 Report level label = 0.01 Pct Recovery = 96% Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl SpecificMix = T1130514013 Laboratory ID = 20140230082 Lab Value = 0.095 Expected Conc. = 0.15 Report level label = 0.01 Pct Recovery = 63% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl SpecificMix = A093651 Laboratory ID = 20132420001 Lab Value = 0.117 Expected Conc. = 0.15 Report level label = 0.01 Pct Recovery = 78% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl SpecificMix = A093651 Laboratory ID = 20130810108 Lab Value = 0.125 Expected Conc. = 0.15 Report level label = 0.01 Pct Recovery = 83% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl SpecificMix = T1120530013 Laboratory ID = 20123560092 Lab Value = 0.114 Expected Conc. = 0.15 Report level label = 0.01 Pct Recovery = 76% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = T1120530013 Laboratory ID = 20131370001 Lab Value = 0.136 Expected Conc. = 0.1255 Report level label = 0.01 Pct Recovery = 108% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl SpecificMix = 1473000 Laboratory ID = 20140370077 Lab Value = 0.089 Expected Conc. = 0.125 Report level label = 0.01 Pct Recovery = 72% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl SpecificMix = T1130514013 Laboratory ID = 20132690010 Lab Value = 0.142 Expected Conc. = 0.125 Report level label = 0.01 Pct Recovery = 114% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl SpecificMix = T1130514013 Laboratory ID = 20161880109 Lab Value = 0.069 Expected Conc. = 0.063 Report level label = 0.01 Pct Recovery = 109% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl SpecificMix = 03FF076 Laboratory ID = 20163370001 Lab Value = 0.063 Expected Conc. = 0.0616 Report level label = 0.01 Pct Recovery = 102% Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl SpecificMix = B20160331 Laboratory ID = 20163150006 Lab Value = 0.059 Expected Conc. = 0.0616 Report level label = 0.01 Pct Recovery = 96% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl SpecificMix = B20160331 Laboratory ID = 20152750006 Lab Value = 0.047 Expected Conc. = 0.06 Report level label = 0.01 Pct Recovery = 78% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl SpecificMix = EN150514012 Laboratory ID = 20152460215 Lab Value = 0.050 Expected Conc. = 0.06 Report level label = 0.01 Pct Recovery = 84% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl SpecificMix = EN150514012 Laboratory ID = 20140860102 Lab Value = 0.036 Expected Conc. = 0.06 Report level label = 0.01 Pct Recovery = 60% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl SpecificMix = A093651 Laboratory ID = 20133400002 Lab Value = 0.049 Expected Conc. = 0.06 Report level label = 0.01 Pct Recovery = 82% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = A093651 Laboratory ID = 20132910008 Lab Value = 0.048 Expected Conc. = 0.06 Report level label = 0.01 Pct Recovery = 80% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = A093651 Laboratory ID = 20131920149 Lab Value = 0.052 Expected Conc. = 0.06 Report level label = 0.01 Pct Recovery = 86% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl SpecificMix = A093651 Laboratory ID = 20131230084 Lab Value = 0.066 Expected Conc. = 0.06 Report level label = 0.01 Pct Recovery = 110% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl SpecificMix = A088380 Laboratory ID = 20130650005 Lab Value = 0.035 Expected Conc. = 0.06 Report level label = 0.01 Pct Recovery = 58% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl SpecificMix = A088380 Laboratory ID = 20130390105 Lab Value = 0.035 Expected Conc. = 0.06 Report level label = 0.01 Pct Recovery = 58% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl SpecificMix = T1120530013 Laboratory ID = 20170960001 Lab Value = 0.045 Expected Conc. = 0.0504 Report level label = 0.01 Pct Recovery = 89% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl SpecificMix = 03FF076 Laboratory ID = 20140730138 Lab Value = 0.042 Expected Conc. = 0.0502 Report level label = 0.01 Pct Recovery = 83% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 1473000 Laboratory ID = 20133470008 Lab Value = 0.048 Expected Conc. = 0.0502 Report level label = 0.01 Pct Recovery = 95% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl SpecificMix = 1473000 Laboratory ID = 20133310030 Lab Value = 0.051 Expected Conc. = 0.0502 Report level label = 0.01 Pct Recovery = 101% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl SpecificMix = 1473000 Laboratory ID = 20131790009 Lab Value = 0.059 Expected Conc. = 0.0502 Report level label = 0.01 Pct Recovery = 118% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl SpecificMix = 1473000 Laboratory ID = 20131650073 Lab Value = 0.056 Expected Conc. = 0.0502 Report level label = 0.01 Pct Recovery = 112% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl SpecificMix = 1473000 Laboratory ID = 20133050050 Lab Value = 0.053 Expected Conc. = 0.05 Report level label = 0.01 Pct Recovery = 106% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl SpecificMix = T1130514013 Laboratory ID = 20132280016 Lab Value = 0.050 Expected Conc. = 0.05 Report level label = 0.01 Pct Recovery = 99% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl SpecificMix = T1130514013 Laboratory ID = 20171720140 Lab Value = 0.063 Expected Conc. = 0.0493 Report level label = 0.01 Pct Recovery = 127% Analysis Date = 08/31/17 SpikeMix = Supelco LC20138V: 80 µl & Phenova B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20171660002 Lab Value = 0.056 Expected Conc. = 0.0493 Report level label = 0.01 Pct Recovery = 113% Analysis Date = 08/23/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20170190026 Lab Value = 0.047 Expected Conc. = 0.0493 Report level label = 0.01 Pct Recovery = 96% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20161470001 Lab Value = 0.054 Expected Conc. = 0.0493 Report level label = 0.01 Pct Recovery = 110% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20142720002 Lab Value = 0.030 Expected Conc. = 0.0402 Report level label = 0.01 Pct Recovery = 74% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl SpecificMix = LC06435 Laboratory ID = 20142530087 Lab Value = 0.025 Expected Conc. = 0.0402 Report level label = 0.01 Pct Recovery = 63% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl SpecificMix = LC06435 Laboratory ID = 20141570088 Lab Value = 0.036 Expected Conc. = 0.0402 Report level label = 0.01 Pct Recovery = 89% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl SpecificMix = LC06435 Laboratory ID = 20141220025 Lab Value = 0.041 Expected Conc. = 0.0402 Report level label = 0.01 Pct Recovery = 101% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl SpecificMix = LC06435 Laboratory ID = 20150720069 Lab Value = 0.033 Expected Conc. = 0.0396 Report level label = 0.01 Pct Recovery = 83% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 03DD006 Laboratory ID = 20143110108 Lab Value = 0.025 Expected Conc. = 0.0396 Report level label = 0.01 Pct Recovery = 63% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 03DD006 Laboratory ID = 20142960086 Lab Value = 0.027 Expected Conc. = 0.0396 Report level label = 0.01 Pct Recovery = 67% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 03DD006 Laboratory ID = 20142270001 Lab Value = 0.025 Expected Conc. = 0.0396 Report level label = 0.01 Pct Recovery = 63% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl SpecificMix = 03DD006 Laboratory ID = 20172230001 Lab Value = 0.039 Expected Conc. = 0.035 Report level label = 0.01 Pct Recovery = 112% Analysis Date = 10/19/17 SpikeMix = ChemService 6472100: 50 µl & Abs 071717Pest: 50 µl SpecificMix = 6472100 Laboratory ID = 20172560101 Lab Value = 0.029 Expected Conc. = 0.0337 Report level label = 0.01 Pct Recovery = 85% Analysis Date = 12/22/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6567600: 50 µl SpecificMix = EN170808006 Laboratory ID = 20172370001 Lab Value = 0.028 Expected Conc. = 0.0337 Report level label = 0.01 Pct Recovery = 83% Analysis Date = 11/18/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6537100: 50 µl SpecificMix = EN170808006 Laboratory ID = 20160630046 Lab Value = 0.023 Expected Conc. = 0.03 Report level label = 0.01 Pct Recovery = 75% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = EN150514012 Laboratory ID = 20153440001 Lab Value = 0.023 Expected Conc. = 0.03 Report level label = 0.01 Pct Recovery = 76% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = EN150514012 Laboratory ID = 20152330039 Lab Value = 0.022 Expected Conc. = 0.03 Report level label = 0.01 Pct Recovery = 74% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl SpecificMix = 041415 Laboratory ID = 20151900132 Lab Value = 0.030 Expected Conc. = 0.03 Report level label = 0.01 Pct Recovery = 100% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl SpecificMix = 041415 Laboratory ID = 20151270112 Lab Value = 0.027 Expected Conc. = 0.03 Report level label = 0.01 Pct Recovery = 88% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl SpecificMix = 041415 Laboratory ID = 20172020035 Lab Value = 0.032 Expected Conc. = 0.0252 Report level label = 0.01 Pct Recovery = 127% Analysis Date = 11/07/17 SpikeMix = Abs 071717Pest: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20171510080 Lab Value = 0.033 Expected Conc. = 0.0252 Report level label = 0.01 Pct Recovery = 129% Analysis Date = 06/09/17 SpikeMix = Supelco LC20138V: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20170460061 Lab Value = 0.025 Expected Conc. = 0.0252 Report level label = 0.01 Pct Recovery = 97% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl SpecificMix = 03FF076 Laboratory ID = 20162660005 Lab Value = 0.021 Expected Conc. = 0.0252 Report level label = 0.01 Pct Recovery = 83% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl SpecificMix = 03FF076 Laboratory ID = 20161600087 Lab Value = 0.026 Expected Conc. = 0.0252 Report level label = 0.01 Pct Recovery = 101% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20161340228 Lab Value = 0.022 Expected Conc. = 0.0252 Report level label = 0.01 Pct Recovery = 87% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl SpecificMix = 03FF076 Laboratory ID = 20161190075 Lab Value = 0.021 Expected Conc. = 0.0252 Report level label = 0.01 Pct Recovery = 85% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20171160110 Lab Value = 0.022 Expected Conc. = 0.0246 Report level label = 0.01 Pct Recovery = 89% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = B20160331 Laboratory ID = 20162380004 Lab Value = 0.024 Expected Conc. = 0.0246 Report level label = 0.01 Pct Recovery = 98% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = B20160331 Laboratory ID = 20162150213 Lab Value = 0.024 Expected Conc. = 0.0246 Report level label = 0.01 Pct Recovery = 98% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl SpecificMix = B20160331 Laboratory ID = 20173120093 Lab Value = 0.027 Expected Conc. = 0.021 Report level label = 0.01 Pct Recovery = 130% Analysis Date = 03/10/18 SpikeMix = ChemService 6472100: 30 µl & ChemService 6537100: 30 µl SpecificMix = 6472100 Laboratory ID = 20150150115 Lab Value = 0.016 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 77% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl SpecificMix = LC06435 Laboratory ID = 20143370094 Lab Value = 0.014 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 67% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl SpecificMix = LC06435 Laboratory ID = 20141910243 Lab Value = 0.016 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 78% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = LC06435 Laboratory ID = 20141840097 Lab Value = 0.016 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 77% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl SpecificMix = LC06435 Laboratory ID = 20142200164 Lab Value = 0.016 Expected Conc. = 0.0198 Report level label = 0.01 Pct Recovery = 79% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 03DD006 Laboratory ID = 20141640076 Lab Value = 0.017 Expected Conc. = 0.0198 Report level label = 0.01 Pct Recovery = 85% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = 03DD006 Laboratory ID = 20141420140 Lab Value = 0.019 Expected Conc. = 0.0198 Report level label = 0.01 Pct Recovery = 94% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 03DD006 Laboratory ID = 20141080004 Lab Value = 0.016 Expected Conc. = 0.0198 Report level label = 0.01 Pct Recovery = 81% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl SpecificMix = 03DD006 Laboratory ID = 20161050143 Lab Value = 0.015 Expected Conc. = 0.015 Report level label = 0.01 Pct Recovery = 98% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 041415 Laboratory ID = 20160560044 Lab Value = 0.012 Expected Conc. = 0.015 Report level label = 0.01 Pct Recovery = 83% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl SpecificMix = 041415 Laboratory ID = 20160210080 Lab Value = 0.012 Expected Conc. = 0.015 Report level label = 0.01 Pct Recovery = 77% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 041415 Laboratory ID = 20160070059 Lab Value = 0.013 Expected Conc. = 0.015 Report level label = 0.01 Pct Recovery = 85% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = EN150514012 Laboratory ID = 20153160001 Lab Value = 0.015 Expected Conc. = 0.015 Report level label = 0.01 Pct Recovery = 100% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = EN150514012 Laboratory ID = 20152950078 Lab Value = 0.010 Expected Conc. = 0.015 Report level label = 0.01 Pct Recovery = 67% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 041415 Laboratory ID = 20152040177 Lab Value = 0.016 Expected Conc. = 0.015 Report level label = 0.01 Pct Recovery = 105% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl SpecificMix = 041415 Laboratory ID = 20151760208 Lab Value = 0.020 Expected Conc. = 0.015 Report level label = 0.01 Pct Recovery = 135% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl SpecificMix = EN150514012 Laboratory ID = 20151480170 Lab Value = 0.013 Expected Conc. = 0.015 Report level label = 0.01 Pct Recovery = 88% Analysis Date = 06/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150514012 Laboratory ID = 20151210037 Lab Value = 0.015 Expected Conc. = 0.015 Report level label = 0.01 Pct Recovery = 99% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 041415 Analysis Date = 03/10/18 Pct Recovery = 112% Analysis Date = 02/28/18 Pct Recovery = 112% Analysis Date = 02/28/18 Pct Recovery = 112% Analysis Date = 02/19/18 Pct Recovery = 112% Analysis Date = 02/19/18 Pct Recovery = 112% Analysis Date = 02/09/18 Pct Recovery = 111% Analysis Date = 02/09/18 Pct Recovery = 111% Analysis Date = 01/31/18 Pct Recovery = 111% Analysis Date = 01/31/18 Pct Recovery = 111% Analysis Date = 01/22/18 Pct Recovery = 111% Analysis Date = 01/22/18 Pct Recovery = 111% Analysis Date = 01/12/18 Pct Recovery = 110% Analysis Date = 01/12/18 Pct Recovery = 110% Analysis Date = 01/03/18 Pct Recovery = 110% Analysis Date = 01/03/18 Pct Recovery = 110% Analysis Date = 12/24/17 Pct Recovery = 110% Analysis Date = 12/24/17 Pct Recovery = 110% Analysis Date = 12/15/17 Pct Recovery = 110% Analysis Date = 12/15/17 Pct Recovery = 110% Analysis Date = 12/06/17 Pct Recovery = 109% Analysis Date = 12/06/17 Pct Recovery = 109% Analysis Date = 11/26/17 Pct Recovery = 109% Analysis Date = 11/26/17 Pct Recovery = 109% Analysis Date = 11/17/17 Pct Recovery = 109% Analysis Date = 11/17/17 Pct Recovery = 109% Analysis Date = 11/07/17 Pct Recovery = 108% Analysis Date = 11/07/17 Pct Recovery = 108% Analysis Date = 10/29/17 Pct Recovery = 108% Analysis Date = 10/29/17 Pct Recovery = 108% Analysis Date = 10/20/17 Pct Recovery = 108% Analysis Date = 10/20/17 Pct Recovery = 108% Analysis Date = 10/10/17 Pct Recovery = 107% Analysis Date = 10/10/17 Pct Recovery = 107% Analysis Date = 10/01/17 Pct Recovery = 107% Analysis Date = 10/01/17 Pct Recovery = 107% Analysis Date = 09/21/17 Pct Recovery = 107% Analysis Date = 09/21/17 Pct Recovery = 107% Analysis Date = 09/12/17 Pct Recovery = 107% Analysis Date = 09/12/17 Pct Recovery = 107% Analysis Date = 09/03/17 Pct Recovery = 106% Analysis Date = 09/03/17 Pct Recovery = 106% Analysis Date = 08/24/17 Pct Recovery = 106% Analysis Date = 08/24/17 Pct Recovery = 106% Analysis Date = 08/15/17 Pct Recovery = 106% Analysis Date = 08/15/17 Pct Recovery = 106% Analysis Date = 08/05/17 Pct Recovery = 105% Analysis Date = 08/05/17 Pct Recovery = 105% Analysis Date = 07/27/17 Pct Recovery = 105% Analysis Date = 07/27/17 Pct Recovery = 105% Analysis Date = 07/18/17 Pct Recovery = 105% Analysis Date = 07/18/17 Pct Recovery = 105% Analysis Date = 07/08/17 Pct Recovery = 104% Analysis Date = 07/08/17 Pct Recovery = 104% Analysis Date = 06/29/17 Pct Recovery = 104% Analysis Date = 06/29/17 Pct Recovery = 104% Analysis Date = 06/19/17 Pct Recovery = 104% Analysis Date = 06/19/17 Pct Recovery = 104% Analysis Date = 06/10/17 Pct Recovery = 103% Analysis Date = 06/10/17 Pct Recovery = 103% Analysis Date = 06/01/17 Pct Recovery = 103% Analysis Date = 06/01/17 Pct Recovery = 103% Analysis Date = 05/22/17 Pct Recovery = 103% Analysis Date = 05/22/17 Pct Recovery = 103% Analysis Date = 05/13/17 Pct Recovery = 103% Analysis Date = 05/13/17 Pct Recovery = 103% Analysis Date = 05/03/17 Pct Recovery = 102% Analysis Date = 05/03/17 Pct Recovery = 102% Analysis Date = 04/24/17 Pct Recovery = 102% Analysis Date = 04/24/17 Pct Recovery = 102% Analysis Date = 04/15/17 Pct Recovery = 102% Analysis Date = 04/15/17 Pct Recovery = 102% Analysis Date = 04/05/17 Pct Recovery = 101% Analysis Date = 04/05/17 Pct Recovery = 101% Analysis Date = 03/27/17 Pct Recovery = 101% Analysis Date = 03/27/17 Pct Recovery = 101% Analysis Date = 03/17/17 Pct Recovery = 101% Analysis Date = 03/17/17 Pct Recovery = 101% Analysis Date = 03/08/17 Pct Recovery = 101% Analysis Date = 03/08/17 Pct Recovery = 101% Analysis Date = 02/27/17 Pct Recovery = 100% Analysis Date = 02/27/17 Pct Recovery = 100% Analysis Date = 02/17/17 Pct Recovery = 100% Analysis Date = 02/17/17 Pct Recovery = 100% Analysis Date = 02/08/17 Pct Recovery = 100% Analysis Date = 02/08/17 Pct Recovery = 100% Analysis Date = 01/29/17 Pct Recovery = 99% Analysis Date = 01/29/17 Pct Recovery = 99% Analysis Date = 01/20/17 Pct Recovery = 99% Analysis Date = 01/20/17 Pct Recovery = 99% Analysis Date = 01/11/17 Pct Recovery = 99% Analysis Date = 01/11/17 Pct Recovery = 99% Analysis Date = 01/01/17 Pct Recovery = 99% Analysis Date = 01/01/17 Pct Recovery = 99% Analysis Date = 12/23/16 Pct Recovery = 98% Analysis Date = 12/23/16 Pct Recovery = 98% Analysis Date = 12/13/16 Pct Recovery = 98% Analysis Date = 12/13/16 Pct Recovery = 98% Analysis Date = 12/04/16 Pct Recovery = 98% Analysis Date = 12/04/16 Pct Recovery = 98% Analysis Date = 11/25/16 Pct Recovery = 97% Analysis Date = 11/25/16 Pct Recovery = 97% Analysis Date = 11/15/16 Pct Recovery = 97% Analysis Date = 11/15/16 Pct Recovery = 97% Analysis Date = 11/06/16 Pct Recovery = 97% Analysis Date = 11/06/16 Pct Recovery = 97% Analysis Date = 10/27/16 Pct Recovery = 97% Analysis Date = 10/27/16 Pct Recovery = 97% Analysis Date = 10/18/16 Pct Recovery = 96% Analysis Date = 10/18/16 Pct Recovery = 96% Analysis Date = 10/09/16 Pct Recovery = 96% Analysis Date = 10/09/16 Pct Recovery = 96% Analysis Date = 09/29/16 Pct Recovery = 96% Analysis Date = 09/29/16 Pct Recovery = 96% Analysis Date = 09/20/16 Pct Recovery = 96% Analysis Date = 09/20/16 Pct Recovery = 96% Analysis Date = 09/10/16 Pct Recovery = 95% Analysis Date = 09/10/16 Pct Recovery = 95% Analysis Date = 09/01/16 Pct Recovery = 95% Analysis Date = 09/01/16 Pct Recovery = 95% Analysis Date = 08/23/16 Pct Recovery = 95% Analysis Date = 08/23/16 Pct Recovery = 95% Analysis Date = 08/13/16 Pct Recovery = 95% Analysis Date = 08/13/16 Pct Recovery = 95% Analysis Date = 08/04/16 Pct Recovery = 94% Analysis Date = 08/04/16 Pct Recovery = 94% Analysis Date = 07/25/16 Pct Recovery = 94% Analysis Date = 07/25/16 Pct Recovery = 94% Analysis Date = 07/16/16 Pct Recovery = 94% Analysis Date = 07/16/16 Pct Recovery = 94% Analysis Date = 07/07/16 Pct Recovery = 94% Analysis Date = 07/07/16 Pct Recovery = 94% Analysis Date = 06/27/16 Pct Recovery = 93% Analysis Date = 06/27/16 Pct Recovery = 93% Analysis Date = 06/18/16 Pct Recovery = 93% Analysis Date = 06/18/16 Pct Recovery = 93% Analysis Date = 06/08/16 Pct Recovery = 93% Analysis Date = 06/08/16 Pct Recovery = 93% Analysis Date = 05/30/16 Pct Recovery = 93% Analysis Date = 05/30/16 Pct Recovery = 93% Analysis Date = 05/21/16 Pct Recovery = 92% Analysis Date = 05/21/16 Pct Recovery = 92% Analysis Date = 05/11/16 Pct Recovery = 92% Analysis Date = 05/11/16 Pct Recovery = 92% Analysis Date = 05/02/16 Pct Recovery = 92% Analysis Date = 05/02/16 Pct Recovery = 92% Analysis Date = 04/22/16 Pct Recovery = 92% Analysis Date = 04/22/16 Pct Recovery = 92% Analysis Date = 04/13/16 Pct Recovery = 91% Analysis Date = 04/13/16 Pct Recovery = 91% Analysis Date = 04/04/16 Pct Recovery = 91% Analysis Date = 04/04/16 Pct Recovery = 91% Analysis Date = 03/25/16 Pct Recovery = 91% Analysis Date = 03/25/16 Pct Recovery = 91% Analysis Date = 03/16/16 Pct Recovery = 91% Analysis Date = 03/16/16 Pct Recovery = 91% Analysis Date = 03/06/16 Pct Recovery = 91% Analysis Date = 03/06/16 Pct Recovery = 91% Analysis Date = 02/26/16 Pct Recovery = 90% Analysis Date = 02/26/16 Pct Recovery = 90% Analysis Date = 02/17/16 Pct Recovery = 90% Analysis Date = 02/17/16 Pct Recovery = 90% Analysis Date = 02/07/16 Pct Recovery = 90% Analysis Date = 02/07/16 Pct Recovery = 90% Analysis Date = 01/29/16 Pct Recovery = 90% Analysis Date = 01/29/16 Pct Recovery = 90% Analysis Date = 01/19/16 Pct Recovery = 90% Analysis Date = 01/19/16 Pct Recovery = 90% Analysis Date = 01/10/16 Pct Recovery = 89% Analysis Date = 01/10/16 Pct Recovery = 89% Analysis Date = 01/01/16 Pct Recovery = 89% Analysis Date = 01/01/16 Pct Recovery = 89% Analysis Date = 12/22/15 Pct Recovery = 89% Analysis Date = 12/22/15 Pct Recovery = 89% Analysis Date = 12/13/15 Pct Recovery = 89% Analysis Date = 12/13/15 Pct Recovery = 89% Analysis Date = 12/03/15 Pct Recovery = 88% Analysis Date = 12/03/15 Pct Recovery = 88% Analysis Date = 11/24/15 Pct Recovery = 88% Analysis Date = 11/24/15 Pct Recovery = 88% Analysis Date = 11/15/15 Pct Recovery = 88% Analysis Date = 11/15/15 Pct Recovery = 88% Analysis Date = 11/05/15 Pct Recovery = 88% Analysis Date = 11/05/15 Pct Recovery = 88% Analysis Date = 10/27/15 Pct Recovery = 88% Analysis Date = 10/27/15 Pct Recovery = 88% Analysis Date = 10/17/15 Pct Recovery = 87% Analysis Date = 10/17/15 Pct Recovery = 87% Analysis Date = 10/08/15 Pct Recovery = 87% Analysis Date = 10/08/15 Pct Recovery = 87% Analysis Date = 09/29/15 Pct Recovery = 87% Analysis Date = 09/29/15 Pct Recovery = 87% Analysis Date = 09/19/15 Pct Recovery = 87% Analysis Date = 09/19/15 Pct Recovery = 87% Analysis Date = 09/10/15 Pct Recovery = 86% Analysis Date = 09/10/15 Pct Recovery = 86% Analysis Date = 08/31/15 Pct Recovery = 86% Analysis Date = 08/31/15 Pct Recovery = 86% Analysis Date = 08/22/15 Pct Recovery = 86% Analysis Date = 08/22/15 Pct Recovery = 86% Analysis Date = 08/13/15 Pct Recovery = 86% Analysis Date = 08/13/15 Pct Recovery = 86% Analysis Date = 08/03/15 Pct Recovery = 85% Analysis Date = 08/03/15 Pct Recovery = 85% Analysis Date = 07/25/15 Pct Recovery = 85% Analysis Date = 07/25/15 Pct Recovery = 85% Analysis Date = 07/15/15 Pct Recovery = 85% Analysis Date = 07/15/15 Pct Recovery = 85% Analysis Date = 07/06/15 Pct Recovery = 85% Analysis Date = 07/06/15 Pct Recovery = 85% Analysis Date = 06/27/15 Pct Recovery = 85% Analysis Date = 06/27/15 Pct Recovery = 85% Analysis Date = 06/17/15 Pct Recovery = 85% Analysis Date = 06/17/15 Pct Recovery = 85% Analysis Date = 06/08/15 Pct Recovery = 85% Analysis Date = 06/08/15 Pct Recovery = 85% Analysis Date = 05/29/15 Pct Recovery = 84% Analysis Date = 05/29/15 Pct Recovery = 84% Analysis Date = 05/20/15 Pct Recovery = 84% Analysis Date = 05/20/15 Pct Recovery = 84% Analysis Date = 05/11/15 Pct Recovery = 84% Analysis Date = 05/11/15 Pct Recovery = 84% Analysis Date = 05/01/15 Pct Recovery = 84% Analysis Date = 05/01/15 Pct Recovery = 84% Analysis Date = 04/22/15 Pct Recovery = 84% Analysis Date = 04/22/15 Pct Recovery = 84% Analysis Date = 04/12/15 Pct Recovery = 84% Analysis Date = 04/12/15 Pct Recovery = 84% Analysis Date = 04/03/15 Pct Recovery = 84% Analysis Date = 04/03/15 Pct Recovery = 84% Analysis Date = 03/25/15 Pct Recovery = 84% Analysis Date = 03/25/15 Pct Recovery = 84% Analysis Date = 03/15/15 Pct Recovery = 84% Analysis Date = 03/15/15 Pct Recovery = 84% Analysis Date = 03/06/15 Pct Recovery = 84% Analysis Date = 03/06/15 Pct Recovery = 84% Analysis Date = 02/24/15 Pct Recovery = 83% Analysis Date = 02/24/15 Pct Recovery = 83% Analysis Date = 02/15/15 Pct Recovery = 83% Analysis Date = 02/15/15 Pct Recovery = 83% Analysis Date = 02/06/15 Pct Recovery = 83% Analysis Date = 02/06/15 Pct Recovery = 83% Analysis Date = 01/27/15 Pct Recovery = 83% Analysis Date = 01/27/15 Pct Recovery = 83% Analysis Date = 01/18/15 Pct Recovery = 83% Analysis Date = 01/18/15 Pct Recovery = 83% Analysis Date = 01/08/15 Pct Recovery = 83% Analysis Date = 01/08/15 Pct Recovery = 83% Analysis Date = 12/30/14 Pct Recovery = 83% Analysis Date = 12/30/14 Pct Recovery = 83% Analysis Date = 12/21/14 Pct Recovery = 83% Analysis Date = 12/21/14 Pct Recovery = 83% Analysis Date = 12/11/14 Pct Recovery = 83% Analysis Date = 12/11/14 Pct Recovery = 83% Analysis Date = 12/02/14 Pct Recovery = 83% Analysis Date = 12/02/14 Pct Recovery = 83% Analysis Date = 11/22/14 Pct Recovery = 83% Analysis Date = 11/22/14 Pct Recovery = 83% Analysis Date = 11/13/14 Pct Recovery = 83% Analysis Date = 11/13/14 Pct Recovery = 83% Analysis Date = 11/04/14 Pct Recovery = 83% Analysis Date = 11/04/14 Pct Recovery = 83% Analysis Date = 10/25/14 Pct Recovery = 83% Analysis Date = 10/25/14 Pct Recovery = 83% Analysis Date = 10/16/14 Pct Recovery = 82% Analysis Date = 10/16/14 Pct Recovery = 82% Analysis Date = 10/06/14 Pct Recovery = 82% Analysis Date = 10/06/14 Pct Recovery = 82% Analysis Date = 09/27/14 Pct Recovery = 82% Analysis Date = 09/27/14 Pct Recovery = 82% Analysis Date = 09/18/14 Pct Recovery = 82% Analysis Date = 09/18/14 Pct Recovery = 82% Analysis Date = 09/08/14 Pct Recovery = 82% Analysis Date = 09/08/14 Pct Recovery = 82% Analysis Date = 08/30/14 Pct Recovery = 82% Analysis Date = 08/30/14 Pct Recovery = 82% Analysis Date = 08/20/14 Pct Recovery = 82% Analysis Date = 08/20/14 Pct Recovery = 82% Analysis Date = 08/11/14 Pct Recovery = 82% Analysis Date = 08/11/14 Pct Recovery = 82% Analysis Date = 08/02/14 Pct Recovery = 83% Analysis Date = 08/02/14 Pct Recovery = 83% Analysis Date = 07/23/14 Pct Recovery = 83% Analysis Date = 07/23/14 Pct Recovery = 83% Analysis Date = 07/14/14 Pct Recovery = 83% Analysis Date = 07/14/14 Pct Recovery = 83% Analysis Date = 07/04/14 Pct Recovery = 83% Analysis Date = 07/04/14 Pct Recovery = 83% Analysis Date = 06/25/14 Pct Recovery = 83% Analysis Date = 06/25/14 Pct Recovery = 83% Analysis Date = 06/16/14 Pct Recovery = 83% Analysis Date = 06/16/14 Pct Recovery = 83% Analysis Date = 06/06/14 Pct Recovery = 83% Analysis Date = 06/06/14 Pct Recovery = 83% Analysis Date = 05/28/14 Pct Recovery = 83% Analysis Date = 05/28/14 Pct Recovery = 83% Analysis Date = 05/18/14 Pct Recovery = 83% Analysis Date = 05/18/14 Pct Recovery = 83% Analysis Date = 05/09/14 Pct Recovery = 83% Analysis Date = 05/09/14 Pct Recovery = 83% Analysis Date = 04/30/14 Pct Recovery = 83% Analysis Date = 04/30/14 Pct Recovery = 83% Analysis Date = 04/20/14 Pct Recovery = 83% Analysis Date = 04/20/14 Pct Recovery = 83% Analysis Date = 04/11/14 Pct Recovery = 83% Analysis Date = 04/11/14 Pct Recovery = 83% Analysis Date = 04/01/14 Pct Recovery = 84% Analysis Date = 04/01/14 Pct Recovery = 84% Analysis Date = 03/23/14 Pct Recovery = 84% Analysis Date = 03/23/14 Pct Recovery = 84% Analysis Date = 03/14/14 Pct Recovery = 84% Analysis Date = 03/14/14 Pct Recovery = 84% Analysis Date = 03/04/14 Pct Recovery = 84% Analysis Date = 03/04/14 Pct Recovery = 84% Analysis Date = 02/23/14 Pct Recovery = 85% Analysis Date = 02/23/14 Pct Recovery = 85% Analysis Date = 02/13/14 Pct Recovery = 85% Analysis Date = 02/13/14 Pct Recovery = 85% Analysis Date = 02/04/14 Pct Recovery = 85% Analysis Date = 02/04/14 Pct Recovery = 85% Analysis Date = 01/26/14 Pct Recovery = 85% Analysis Date = 01/26/14 Pct Recovery = 85% Analysis Date = 01/16/14 Pct Recovery = 85% Analysis Date = 01/16/14 Pct Recovery = 85% Analysis Date = 01/07/14 Pct Recovery = 86% Analysis Date = 01/07/14 Pct Recovery = 86% Analysis Date = 12/28/13 Pct Recovery = 86% Analysis Date = 12/28/13 Pct Recovery = 86% Analysis Date = 12/19/13 Pct Recovery = 86% Analysis Date = 12/19/13 Pct Recovery = 86% Analysis Date = 12/10/13 Pct Recovery = 86% Analysis Date = 12/10/13 Pct Recovery = 86% Analysis Date = 11/30/13 Pct Recovery = 86% Analysis Date = 11/30/13 Pct Recovery = 86% Analysis Date = 11/21/13 Pct Recovery = 86% Analysis Date = 11/21/13 Pct Recovery = 86% Analysis Date = 11/11/13 Pct Recovery = 86% Analysis Date = 11/11/13 Pct Recovery = 86% Analysis Date = 11/02/13 Pct Recovery = 87% Analysis Date = 11/02/13 Pct Recovery = 87% Analysis Date = 10/24/13 Pct Recovery = 87% Analysis Date = 10/24/13 Pct Recovery = 87% Analysis Date = 10/14/13 Pct Recovery = 87% Analysis Date = 10/14/13 Pct Recovery = 87% Analysis Date = 10/05/13 Pct Recovery = 87% Analysis Date = 10/05/13 Pct Recovery = 87% Analysis Date = 09/25/13 Pct Recovery = 87% Analysis Date = 09/25/13 Pct Recovery = 87% Analysis Date = 09/16/13 Pct Recovery = 87% Analysis Date = 09/16/13 Pct Recovery = 87% Analysis Date = 09/07/13 Pct Recovery = 87% Analysis Date = 09/07/13 Pct Recovery = 87% Analysis Date = 08/28/13 Pct Recovery = 88% Analysis Date = 08/28/13 Pct Recovery = 88% Analysis Date = 08/19/13 Pct Recovery = 88% Analysis Date = 08/19/13 Pct Recovery = 88% Analysis Date = 08/09/13 Pct Recovery = 88% Analysis Date = 08/09/13 Pct Recovery = 88% Analysis Date = 07/31/13 Pct Recovery = 88% Analysis Date = 07/31/13 Pct Recovery = 88% Analysis Date = 07/22/13 Pct Recovery = 88% Analysis Date = 07/22/13 Pct Recovery = 88% Analysis Date = 07/12/13 Pct Recovery = 88% Analysis Date = 07/12/13 Pct Recovery = 88% Analysis Date = 07/03/13 Pct Recovery = 88% Analysis Date = 07/03/13 Pct Recovery = 88% Analysis Date = 06/23/13 Pct Recovery = 89% Analysis Date = 06/23/13 Pct Recovery = 89% Analysis Date = 06/14/13 Pct Recovery = 89% Analysis Date = 06/14/13 Pct Recovery = 89% Analysis Date = 06/05/13 Pct Recovery = 89% Analysis Date = 06/05/13 Pct Recovery = 89% Analysis Date = 05/26/13 Pct Recovery = 89% Analysis Date = 05/26/13 Pct Recovery = 89% Analysis Date = 05/17/13 Pct Recovery = 89% Analysis Date = 05/17/13 Pct Recovery = 89% Analysis Date = 05/07/13 Pct Recovery = 89% Analysis Date = 05/07/13 Pct Recovery = 89% Analysis Date = 04/28/13 Pct Recovery = 89% Analysis Date = 04/28/13 Pct Recovery = 89% Analysis Date = 04/19/13 Pct Recovery = 90% Analysis Date = 04/19/13 Pct Recovery = 90% Analysis Date = 04/09/13 Pct Recovery = 90% Analysis Date = 04/09/13 Pct Recovery = 90% Analysis Date = 03/31/13 Pct Recovery = 90% Analysis Date = 03/31/13 Pct Recovery = 90% Analysis Date = 03/21/13 Pct Recovery = 90% Analysis Date = 03/21/13 Pct Recovery = 90% Analysis Date = 03/12/13 Pct Recovery = 90% Analysis Date = 03/12/13 Pct Recovery = 90% Analysis Date = 03/03/13 Pct Recovery = 90% Analysis Date = 03/03/13 Pct Recovery = 90% Analysis Date = 02/21/13 Pct Recovery = 90% Analysis Date = 02/21/13 Pct Recovery = 90% Analysis Date = 02/12/13 Pct Recovery = 90% Analysis Date = 02/12/13 Pct Recovery = 90% Analysis Date = 02/02/13 Pct Recovery = 91% Analysis Date = 02/02/13 Pct Recovery = 91% Analysis Date = 01/24/13 Pct Recovery = 91% Analysis Date = 01/24/13 Pct Recovery = 91% Analysis Date = 01/15/13 Pct Recovery = 91% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
ACETOCHLOR

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 79 90% 18% 87% 18%
Total 79 90% 18% 87% 18%

Sample Statistics
ACETOCHLOR

Characteristic N % % Basis
Plotted 79 100% Spiked
Estimated Values 5 6% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 79 .  
False Negatives 0 0% 0 out of 79
Not Spiked 39 .  
False Positives 0 0% 0 out of 39

OBSP Determination:
ALACHLOR
METHOD: 2033 , TESTIDCODE: 46342GCM35

Laboratory ID = 20130250061 Lab Value = 0.126 Expected Conc. = 0.15 Report level label = 0.008 Pct Recovery = 84% Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl SpecificMix = A088380 Laboratory ID = 20140230082 Lab Value = 0.057 Expected Conc. = 0.075 Report level label = 0.008 Pct Recovery = 76% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl SpecificMix = A093651 Laboratory ID = 20132420001 Lab Value = 0.065 Expected Conc. = 0.075 Report level label = 0.008 Pct Recovery = 86% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl SpecificMix = A093651 Laboratory ID = 20130810108 Lab Value = 0.067 Expected Conc. = 0.075 Report level label = 0.008 Pct Recovery = 89% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl SpecificMix = T1120530013 Laboratory ID = 20123560092 Lab Value = 0.063 Expected Conc. = 0.075 Report level label = 0.008 Pct Recovery = 85% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = T1120530013 Laboratory ID = 20140100085 Lab Value = 0.072 Expected Conc. = 0.07 Report level label = 0.008 Pct Recovery = 102% Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl SpecificMix = T1130514013 Laboratory ID = 20132490342 Lab Value = 0.079 Expected Conc. = 0.07 Report level label = 0.008 Pct Recovery = 113% Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl SpecificMix = T1130514013 Laboratory ID = 20172510330 Lab Value = 0.045 Expected Conc. = 0.053 Report level label = 0.008 Pct Recovery = 86% Analysis Date = 12/29/17 SpikeMix = ChemService 6537100: 100 µl & Abs 071817Pest: 100 µl SpecificMix = 6537100 Laboratory ID = 20162860079 Lab Value = 0.057 Expected Conc. = 0.05 Report level label = 0.008 Pct Recovery = 114% Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl SpecificMix = 060916 Laboratory ID = 20163150006 Lab Value = 0.049 Expected Conc. = 0.05 Report level label = 0.008 Pct Recovery = 99% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl SpecificMix = 060916 Laboratory ID = 20152750006 Lab Value = 0.037 Expected Conc. = 0.048 Report level label = 0.008 Pct Recovery = 77% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl SpecificMix = EN150514012 Laboratory ID = 20152460215 Lab Value = 0.045 Expected Conc. = 0.048 Report level label = 0.008 Pct Recovery = 93% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl SpecificMix = EN150514012 Laboratory ID = 20171660002 Lab Value = 0.041 Expected Conc. = 0.04 Report level label = 0.008 Pct Recovery = 102% Analysis Date = 08/23/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = 060916 Laboratory ID = 20171380001 Lab Value = 0.028 Expected Conc. = 0.04 Report level label = 0.008 Pct Recovery = 70% Analysis Date = 06/07/17 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 041816 Laboratory ID = 20170740063 Lab Value = 0.038 Expected Conc. = 0.04 Report level label = 0.008 Pct Recovery = 94% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl SpecificMix = 041816 Laboratory ID = 20170190026 Lab Value = 0.038 Expected Conc. = 0.04 Report level label = 0.008 Pct Recovery = 96% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = 060916 Laboratory ID = 20161740258 Lab Value = 0.025 Expected Conc. = 0.04 Report level label = 0.008 Pct Recovery = 63% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 041816 Laboratory ID = 20140370077 Lab Value = 0.030 Expected Conc. = 0.035 Report level label = 0.008 Pct Recovery = 84% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl SpecificMix = T1130514013 Laboratory ID = 20132690010 Lab Value = 0.046 Expected Conc. = 0.035 Report level label = 0.008 Pct Recovery = 131% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl SpecificMix = T1130514013 Laboratory ID = 20131370001 Lab Value = 0.038 Expected Conc. = 0.035 Report level label = 0.008 Pct Recovery = 109% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl SpecificMix = 1473000 Laboratory ID = 20142720002 Lab Value = 0.026 Expected Conc. = 0.0319 Report level label = 0.008 Pct Recovery = 80% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl SpecificMix = LC06435 Laboratory ID = 20142530087 Lab Value = 0.024 Expected Conc. = 0.0319 Report level label = 0.008 Pct Recovery = 76% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl SpecificMix = LC06435 Laboratory ID = 20141570088 Lab Value = 0.031 Expected Conc. = 0.0319 Report level label = 0.008 Pct Recovery = 97% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl SpecificMix = LC06435 Laboratory ID = 20141220025 Lab Value = 0.034 Expected Conc. = 0.0319 Report level label = 0.008 Pct Recovery = 107% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl SpecificMix = LC06435 Laboratory ID = 20150720069 Lab Value = 0.031 Expected Conc. = 0.0318 Report level label = 0.008 Pct Recovery = 99% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 03DD006 Laboratory ID = 20143110108 Lab Value = 0.026 Expected Conc. = 0.0318 Report level label = 0.008 Pct Recovery = 81% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 03DD006 Laboratory ID = 20142960086 Lab Value = 0.027 Expected Conc. = 0.0318 Report level label = 0.008 Pct Recovery = 83% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 03DD006 Laboratory ID = 20142270001 Lab Value = 0.023 Expected Conc. = 0.0318 Report level label = 0.008 Pct Recovery = 73% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl SpecificMix = 03DD006 Laboratory ID = 20140860102 Lab Value = 0.022 Expected Conc. = 0.03 Report level label = 0.008 Pct Recovery = 72% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl SpecificMix = A093651 Laboratory ID = 20133400002 Lab Value = 0.027 Expected Conc. = 0.03 Report level label = 0.008 Pct Recovery = 91% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = A093651 Laboratory ID = 20132910008 Lab Value = 0.027 Expected Conc. = 0.03 Report level label = 0.008 Pct Recovery = 89% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = A093651 Laboratory ID = 20131920149 Lab Value = 0.028 Expected Conc. = 0.03 Report level label = 0.008 Pct Recovery = 93% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl SpecificMix = A093651 Laboratory ID = 20131230084 Lab Value = 0.033 Expected Conc. = 0.03 Report level label = 0.008 Pct Recovery = 111% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl SpecificMix = A088380 Laboratory ID = 20130650005 Lab Value = 0.021 Expected Conc. = 0.03 Report level label = 0.008 Pct Recovery = 69% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl SpecificMix = A088380 Laboratory ID = 20130390105 Lab Value = 0.021 Expected Conc. = 0.03 Report level label = 0.008 Pct Recovery = 69% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl SpecificMix = T1120530013 Laboratory ID = 20172370001 Lab Value = 0.024 Expected Conc. = 0.0265 Report level label = 0.008 Pct Recovery = 92% Analysis Date = 11/18/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6537100: 50 µl SpecificMix = 6537100 Laboratory ID = 20172230001 Lab Value = 0.033 Expected Conc. = 0.0265 Report level label = 0.008 Pct Recovery = 124% Analysis Date = 10/19/17 SpikeMix = ChemService 6472100: 50 µl & Abs 071717Pest: 50 µl SpecificMix = 071717Pest Laboratory ID = 20160630046 Lab Value = 0.018 Expected Conc. = 0.024 Report level label = 0.008 Pct Recovery = 75% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = EN150514012 Laboratory ID = 20153440001 Lab Value = 0.018 Expected Conc. = 0.024 Report level label = 0.008 Pct Recovery = 76% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = EN150514012 Laboratory ID = 20152330039 Lab Value = 0.021 Expected Conc. = 0.024 Report level label = 0.008 Pct Recovery = 87% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl SpecificMix = 041415 Laboratory ID = 20151900132 Lab Value = 0.024 Expected Conc. = 0.024 Report level label = 0.008 Pct Recovery = 101% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl SpecificMix = 041415 Laboratory ID = 20151270112 Lab Value = 0.024 Expected Conc. = 0.024 Report level label = 0.008 Pct Recovery = 100% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl SpecificMix = 041415 Laboratory ID = 20172020035 Lab Value = 0.027 Expected Conc. = 0.0212 Report level label = 0.008 Pct Recovery = 125% Analysis Date = 11/07/17 SpikeMix = Abs 071717Pest: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 071717Pest Laboratory ID = 20171940002 Lab Value = 0.018 Expected Conc. = 0.02 Report level label = 0.008 Pct Recovery = 92% Analysis Date = 11/10/17 SpikeMix = ChemService 5054800: 40 µl & NSI 041816: 40 µl SpecificMix = 041816 Laboratory ID = 20171160110 Lab Value = 0.019 Expected Conc. = 0.02 Report level label = 0.008 Pct Recovery = 96% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = 060916 Laboratory ID = 20162520001 Lab Value = 0.025 Expected Conc. = 0.02 Report level label = 0.008 Pct Recovery = 125% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl SpecificMix = 060916 Laboratory ID = 20163560019 Lab Value = 0.020 Expected Conc. = 0.02 Report level label = 0.008 Pct Recovery = 101% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl SpecificMix = 060916 Laboratory ID = 20162380004 Lab Value = 0.020 Expected Conc. = 0.02 Report level label = 0.008 Pct Recovery = 101% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = 060916 Laboratory ID = 20162020124 Lab Value = 0.017 Expected Conc. = 0.02 Report level label = 0.008 Pct Recovery = 85% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl SpecificMix = 041816 Laboratory ID = 20161600087 Lab Value = 0.019 Expected Conc. = 0.02 Report level label = 0.008 Pct Recovery = 96% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 041816 Laboratory ID = 20161340228 Lab Value = 0.017 Expected Conc. = 0.02 Report level label = 0.008 Pct Recovery = 84% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl SpecificMix = 041816 Laboratory ID = 20161190075 Lab Value = 0.016 Expected Conc. = 0.02 Report level label = 0.008 Pct Recovery = 82% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 041816 Laboratory ID = 20150150115 Lab Value = 0.013 Expected Conc. = 0.016 Report level label = 0.008 Pct Recovery = 83% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl SpecificMix = LC06435 Laboratory ID = 20143370094 Lab Value = 0.012 Expected Conc. = 0.016 Report level label = 0.008 Pct Recovery = 76% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl SpecificMix = LC06435 Laboratory ID = 20141910243 Lab Value = 0.013 Expected Conc. = 0.016 Report level label = 0.008 Pct Recovery = 81% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = LC06435 Laboratory ID = 20141840097 Lab Value = 0.013 Expected Conc. = 0.016 Report level label = 0.008 Pct Recovery = 82% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl SpecificMix = LC06435 Laboratory ID = 20173120093 Lab Value = 0.019 Expected Conc. = 0.0159 Report level label = 0.008 Pct Recovery = 119% Analysis Date = 03/10/18 SpikeMix = ChemService 6472100: 30 µl & ChemService 6537100: 30 µl SpecificMix = 6537100 Laboratory ID = 20142200164 Lab Value = 0.014 Expected Conc. = 0.0159 Report level label = 0.008 Pct Recovery = 90% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 03DD006 Laboratory ID = 20141640076 Lab Value = 0.014 Expected Conc. = 0.0159 Report level label = 0.008 Pct Recovery = 89% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = 03DD006 Laboratory ID = 20141420140 Lab Value = 0.016 Expected Conc. = 0.0159 Report level label = 0.008 Pct Recovery = 102% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 03DD006 Laboratory ID = 20141080004 Lab Value = 0.014 Expected Conc. = 0.0159 Report level label = 0.008 Pct Recovery = 88% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl SpecificMix = 03DD006 Laboratory ID = 20140730138 Lab Value = 0.014 Expected Conc. = 0.014 Report level label = 0.008 Pct Recovery = 101% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 1473000 Laboratory ID = 20133470008 Lab Value = 0.014 Expected Conc. = 0.014 Report level label = 0.008 Pct Recovery = 99% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl SpecificMix = 1473000 Laboratory ID = 20133310030 Lab Value = 0.016 Expected Conc. = 0.014 Report level label = 0.008 Pct Recovery = 113% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl SpecificMix = 1473000 Laboratory ID = 20133050050 Lab Value = 0.017 Expected Conc. = 0.014 Report level label = 0.008 Pct Recovery = 120% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl SpecificMix = T1130514013 Laboratory ID = 20132280016 Lab Value = 0.017 Expected Conc. = 0.014 Report level label = 0.008 Pct Recovery = 119% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl SpecificMix = T1130514013 Laboratory ID = 20131790009 Lab Value = 0.018 Expected Conc. = 0.014 Report level label = 0.008 Pct Recovery = 126% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl SpecificMix = 1473000 Laboratory ID = 20131650073 Lab Value = 0.018 Expected Conc. = 0.014 Report level label = 0.008 Pct Recovery = 130% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl SpecificMix = 1473000 Laboratory ID = 20161050143 Lab Value = 0.013 Expected Conc. = 0.012 Report level label = 0.008 Pct Recovery = 106% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 041415 Laboratory ID = 20160560044 Lab Value = 0.011 Expected Conc. = 0.012 Report level label = 0.008 Pct Recovery = 90% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl SpecificMix = 041415 Laboratory ID = 20160210080 Lab Value = 0.011 Expected Conc. = 0.012 Report level label = 0.008 Pct Recovery = 90% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 041415 Laboratory ID = 20160070059 Lab Value = 0.011 Expected Conc. = 0.012 Report level label = 0.008 Pct Recovery = 95% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = EN150514012 Laboratory ID = 20153160001 Lab Value = 0.011 Expected Conc. = 0.012 Report level label = 0.008 Pct Recovery = 93% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = EN150514012 Laboratory ID = 20152950078 Lab Value = 0.008 Expected Conc. = 0.012 Report level label = 0.008 Pct Recovery = 69% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 041415 Laboratory ID = 20152040177 Lab Value = 0.013 Expected Conc. = 0.012 Report level label = 0.008 Pct Recovery = 104% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl SpecificMix = 041415 Laboratory ID = 20151760208 Lab Value = 0.015 Expected Conc. = 0.012 Report level label = 0.008 Pct Recovery = 124% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl SpecificMix = EN150514012 Laboratory ID = 20151480170 Lab Value = 0.011 Expected Conc. = 0.012 Report level label = 0.008 Pct Recovery = 91% Analysis Date = 06/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150514012 Laboratory ID = 20151210037 Lab Value = 0.013 Expected Conc. = 0.012 Report level label = 0.008 Pct Recovery = 105% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 041415 Analysis Date = 03/10/18 Pct Recovery = 106% Analysis Date = 02/28/18 Pct Recovery = 106% Analysis Date = 02/28/18 Pct Recovery = 106% Analysis Date = 02/19/18 Pct Recovery = 105% Analysis Date = 02/19/18 Pct Recovery = 105% Analysis Date = 02/09/18 Pct Recovery = 105% Analysis Date = 02/09/18 Pct Recovery = 105% Analysis Date = 01/31/18 Pct Recovery = 105% Analysis Date = 01/31/18 Pct Recovery = 105% Analysis Date = 01/22/18 Pct Recovery = 105% Analysis Date = 01/22/18 Pct Recovery = 105% Analysis Date = 01/12/18 Pct Recovery = 105% Analysis Date = 01/12/18 Pct Recovery = 105% Analysis Date = 01/03/18 Pct Recovery = 104% Analysis Date = 01/03/18 Pct Recovery = 104% Analysis Date = 12/24/17 Pct Recovery = 104% Analysis Date = 12/24/17 Pct Recovery = 104% Analysis Date = 12/15/17 Pct Recovery = 104% Analysis Date = 12/15/17 Pct Recovery = 104% Analysis Date = 12/06/17 Pct Recovery = 104% Analysis Date = 12/06/17 Pct Recovery = 104% Analysis Date = 11/26/17 Pct Recovery = 103% Analysis Date = 11/26/17 Pct Recovery = 103% Analysis Date = 11/17/17 Pct Recovery = 103% Analysis Date = 11/17/17 Pct Recovery = 103% Analysis Date = 11/07/17 Pct Recovery = 103% Analysis Date = 11/07/17 Pct Recovery = 103% Analysis Date = 10/29/17 Pct Recovery = 103% Analysis Date = 10/29/17 Pct Recovery = 103% Analysis Date = 10/20/17 Pct Recovery = 103% Analysis Date = 10/20/17 Pct Recovery = 103% Analysis Date = 10/10/17 Pct Recovery = 102% Analysis Date = 10/10/17 Pct Recovery = 102% Analysis Date = 10/01/17 Pct Recovery = 102% Analysis Date = 10/01/17 Pct Recovery = 102% Analysis Date = 09/21/17 Pct Recovery = 102% Analysis Date = 09/21/17 Pct Recovery = 102% Analysis Date = 09/12/17 Pct Recovery = 102% Analysis Date = 09/12/17 Pct Recovery = 102% Analysis Date = 09/03/17 Pct Recovery = 101% Analysis Date = 09/03/17 Pct Recovery = 101% Analysis Date = 08/24/17 Pct Recovery = 101% Analysis Date = 08/24/17 Pct Recovery = 101% Analysis Date = 08/15/17 Pct Recovery = 101% Analysis Date = 08/15/17 Pct Recovery = 101% Analysis Date = 08/05/17 Pct Recovery = 101% Analysis Date = 08/05/17 Pct Recovery = 101% Analysis Date = 07/27/17 Pct Recovery = 101% Analysis Date = 07/27/17 Pct Recovery = 101% Analysis Date = 07/18/17 Pct Recovery = 100% Analysis Date = 07/18/17 Pct Recovery = 100% Analysis Date = 07/08/17 Pct Recovery = 100% Analysis Date = 07/08/17 Pct Recovery = 100% Analysis Date = 06/29/17 Pct Recovery = 100% Analysis Date = 06/29/17 Pct Recovery = 100% Analysis Date = 06/19/17 Pct Recovery = 100% Analysis Date = 06/19/17 Pct Recovery = 100% Analysis Date = 06/10/17 Pct Recovery = 99% Analysis Date = 06/10/17 Pct Recovery = 99% Analysis Date = 06/01/17 Pct Recovery = 99% Analysis Date = 06/01/17 Pct Recovery = 99% Analysis Date = 05/22/17 Pct Recovery = 99% Analysis Date = 05/22/17 Pct Recovery = 99% Analysis Date = 05/13/17 Pct Recovery = 99% Analysis Date = 05/13/17 Pct Recovery = 99% Analysis Date = 05/03/17 Pct Recovery = 99% Analysis Date = 05/03/17 Pct Recovery = 99% Analysis Date = 04/24/17 Pct Recovery = 98% Analysis Date = 04/24/17 Pct Recovery = 98% Analysis Date = 04/15/17 Pct Recovery = 98% Analysis Date = 04/15/17 Pct Recovery = 98% Analysis Date = 04/05/17 Pct Recovery = 98% Analysis Date = 04/05/17 Pct Recovery = 98% Analysis Date = 03/27/17 Pct Recovery = 98% Analysis Date = 03/27/17 Pct Recovery = 98% Analysis Date = 03/17/17 Pct Recovery = 97% Analysis Date = 03/17/17 Pct Recovery = 97% Analysis Date = 03/08/17 Pct Recovery = 97% Analysis Date = 03/08/17 Pct Recovery = 97% Analysis Date = 02/27/17 Pct Recovery = 97% Analysis Date = 02/27/17 Pct Recovery = 97% Analysis Date = 02/17/17 Pct Recovery = 97% Analysis Date = 02/17/17 Pct Recovery = 97% Analysis Date = 02/08/17 Pct Recovery = 97% Analysis Date = 02/08/17 Pct Recovery = 97% Analysis Date = 01/29/17 Pct Recovery = 97% Analysis Date = 01/29/17 Pct Recovery = 97% Analysis Date = 01/20/17 Pct Recovery = 96% Analysis Date = 01/20/17 Pct Recovery = 96% Analysis Date = 01/11/17 Pct Recovery = 96% Analysis Date = 01/11/17 Pct Recovery = 96% Analysis Date = 01/01/17 Pct Recovery = 96% Analysis Date = 01/01/17 Pct Recovery = 96% Analysis Date = 12/23/16 Pct Recovery = 96% Analysis Date = 12/23/16 Pct Recovery = 96% Analysis Date = 12/13/16 Pct Recovery = 96% Analysis Date = 12/13/16 Pct Recovery = 96% Analysis Date = 12/04/16 Pct Recovery = 96% Analysis Date = 12/04/16 Pct Recovery = 96% Analysis Date = 11/25/16 Pct Recovery = 95% Analysis Date = 11/25/16 Pct Recovery = 95% Analysis Date = 11/15/16 Pct Recovery = 95% Analysis Date = 11/15/16 Pct Recovery = 95% Analysis Date = 11/06/16 Pct Recovery = 95% Analysis Date = 11/06/16 Pct Recovery = 95% Analysis Date = 10/27/16 Pct Recovery = 95% Analysis Date = 10/27/16 Pct Recovery = 95% Analysis Date = 10/18/16 Pct Recovery = 95% Analysis Date = 10/18/16 Pct Recovery = 95% Analysis Date = 10/09/16 Pct Recovery = 95% Analysis Date = 10/09/16 Pct Recovery = 95% Analysis Date = 09/29/16 Pct Recovery = 94% Analysis Date = 09/29/16 Pct Recovery = 94% Analysis Date = 09/20/16 Pct Recovery = 94% Analysis Date = 09/20/16 Pct Recovery = 94% Analysis Date = 09/10/16 Pct Recovery = 94% Analysis Date = 09/10/16 Pct Recovery = 94% Analysis Date = 09/01/16 Pct Recovery = 94% Analysis Date = 09/01/16 Pct Recovery = 94% Analysis Date = 08/23/16 Pct Recovery = 94% Analysis Date = 08/23/16 Pct Recovery = 94% Analysis Date = 08/13/16 Pct Recovery = 94% Analysis Date = 08/13/16 Pct Recovery = 94% Analysis Date = 08/04/16 Pct Recovery = 93% Analysis Date = 08/04/16 Pct Recovery = 93% Analysis Date = 07/25/16 Pct Recovery = 93% Analysis Date = 07/25/16 Pct Recovery = 93% Analysis Date = 07/16/16 Pct Recovery = 93% Analysis Date = 07/16/16 Pct Recovery = 93% Analysis Date = 07/07/16 Pct Recovery = 93% Analysis Date = 07/07/16 Pct Recovery = 93% Analysis Date = 06/27/16 Pct Recovery = 93% Analysis Date = 06/27/16 Pct Recovery = 93% Analysis Date = 06/18/16 Pct Recovery = 93% Analysis Date = 06/18/16 Pct Recovery = 93% Analysis Date = 06/08/16 Pct Recovery = 92% Analysis Date = 06/08/16 Pct Recovery = 92% Analysis Date = 05/30/16 Pct Recovery = 92% Analysis Date = 05/30/16 Pct Recovery = 92% Analysis Date = 05/21/16 Pct Recovery = 92% Analysis Date = 05/21/16 Pct Recovery = 92% Analysis Date = 05/11/16 Pct Recovery = 92% Analysis Date = 05/11/16 Pct Recovery = 92% Analysis Date = 05/02/16 Pct Recovery = 92% Analysis Date = 05/02/16 Pct Recovery = 92% Analysis Date = 04/22/16 Pct Recovery = 92% Analysis Date = 04/22/16 Pct Recovery = 92% Analysis Date = 04/13/16 Pct Recovery = 92% Analysis Date = 04/13/16 Pct Recovery = 92% Analysis Date = 04/04/16 Pct Recovery = 92% Analysis Date = 04/04/16 Pct Recovery = 92% Analysis Date = 03/25/16 Pct Recovery = 92% Analysis Date = 03/25/16 Pct Recovery = 92% Analysis Date = 03/16/16 Pct Recovery = 91% Analysis Date = 03/16/16 Pct Recovery = 91% Analysis Date = 03/06/16 Pct Recovery = 91% Analysis Date = 03/06/16 Pct Recovery = 91% Analysis Date = 02/26/16 Pct Recovery = 91% Analysis Date = 02/26/16 Pct Recovery = 91% Analysis Date = 02/17/16 Pct Recovery = 91% Analysis Date = 02/17/16 Pct Recovery = 91% Analysis Date = 02/07/16 Pct Recovery = 91% Analysis Date = 02/07/16 Pct Recovery = 91% Analysis Date = 01/29/16 Pct Recovery = 91% Analysis Date = 01/29/16 Pct Recovery = 91% Analysis Date = 01/19/16 Pct Recovery = 91% Analysis Date = 01/19/16 Pct Recovery = 91% Analysis Date = 01/10/16 Pct Recovery = 91% Analysis Date = 01/10/16 Pct Recovery = 91% Analysis Date = 01/01/16 Pct Recovery = 91% Analysis Date = 01/01/16 Pct Recovery = 91% Analysis Date = 12/22/15 Pct Recovery = 91% Analysis Date = 12/22/15 Pct Recovery = 91% Analysis Date = 12/13/15 Pct Recovery = 91% Analysis Date = 12/13/15 Pct Recovery = 91% Analysis Date = 12/03/15 Pct Recovery = 91% Analysis Date = 12/03/15 Pct Recovery = 91% Analysis Date = 11/24/15 Pct Recovery = 91% Analysis Date = 11/24/15 Pct Recovery = 91% Analysis Date = 11/15/15 Pct Recovery = 90% Analysis Date = 11/15/15 Pct Recovery = 90% Analysis Date = 11/05/15 Pct Recovery = 90% Analysis Date = 11/05/15 Pct Recovery = 90% Analysis Date = 10/27/15 Pct Recovery = 90% Analysis Date = 10/27/15 Pct Recovery = 90% Analysis Date = 10/17/15 Pct Recovery = 90% Analysis Date = 10/17/15 Pct Recovery = 90% Analysis Date = 10/08/15 Pct Recovery = 90% Analysis Date = 10/08/15 Pct Recovery = 90% Analysis Date = 09/29/15 Pct Recovery = 90% Analysis Date = 09/29/15 Pct Recovery = 90% Analysis Date = 09/19/15 Pct Recovery = 90% Analysis Date = 09/19/15 Pct Recovery = 90% Analysis Date = 09/10/15 Pct Recovery = 90% Analysis Date = 09/10/15 Pct Recovery = 90% Analysis Date = 08/31/15 Pct Recovery = 90% Analysis Date = 08/31/15 Pct Recovery = 90% Analysis Date = 08/22/15 Pct Recovery = 90% Analysis Date = 08/22/15 Pct Recovery = 90% Analysis Date = 08/13/15 Pct Recovery = 90% Analysis Date = 08/13/15 Pct Recovery = 90% Analysis Date = 08/03/15 Pct Recovery = 90% Analysis Date = 08/03/15 Pct Recovery = 90% Analysis Date = 07/25/15 Pct Recovery = 90% Analysis Date = 07/25/15 Pct Recovery = 90% Analysis Date = 07/15/15 Pct Recovery = 90% Analysis Date = 07/15/15 Pct Recovery = 90% Analysis Date = 07/06/15 Pct Recovery = 90% Analysis Date = 07/06/15 Pct Recovery = 90% Analysis Date = 06/27/15 Pct Recovery = 90% Analysis Date = 06/27/15 Pct Recovery = 90% Analysis Date = 06/17/15 Pct Recovery = 90% Analysis Date = 06/17/15 Pct Recovery = 90% Analysis Date = 06/08/15 Pct Recovery = 90% Analysis Date = 06/08/15 Pct Recovery = 90% Analysis Date = 05/29/15 Pct Recovery = 90% Analysis Date = 05/29/15 Pct Recovery = 90% Analysis Date = 05/20/15 Pct Recovery = 90% Analysis Date = 05/20/15 Pct Recovery = 90% Analysis Date = 05/11/15 Pct Recovery = 90% Analysis Date = 05/11/15 Pct Recovery = 90% Analysis Date = 05/01/15 Pct Recovery = 90% Analysis Date = 05/01/15 Pct Recovery = 90% Analysis Date = 04/22/15 Pct Recovery = 90% Analysis Date = 04/22/15 Pct Recovery = 90% Analysis Date = 04/12/15 Pct Recovery = 90% Analysis Date = 04/12/15 Pct Recovery = 90% Analysis Date = 04/03/15 Pct Recovery = 91% Analysis Date = 04/03/15 Pct Recovery = 91% Analysis Date = 03/25/15 Pct Recovery = 91% Analysis Date = 03/25/15 Pct Recovery = 91% Analysis Date = 03/15/15 Pct Recovery = 91% Analysis Date = 03/15/15 Pct Recovery = 91% Analysis Date = 03/06/15 Pct Recovery = 91% Analysis Date = 03/06/15 Pct Recovery = 91% Analysis Date = 02/24/15 Pct Recovery = 91% Analysis Date = 02/24/15 Pct Recovery = 91% Analysis Date = 02/15/15 Pct Recovery = 91% Analysis Date = 02/15/15 Pct Recovery = 91% Analysis Date = 02/06/15 Pct Recovery = 91% Analysis Date = 02/06/15 Pct Recovery = 91% Analysis Date = 01/27/15 Pct Recovery = 91% Analysis Date = 01/27/15 Pct Recovery = 91% Analysis Date = 01/18/15 Pct Recovery = 91% Analysis Date = 01/18/15 Pct Recovery = 91% Analysis Date = 01/08/15 Pct Recovery = 91% Analysis Date = 01/08/15 Pct Recovery = 91% Analysis Date = 12/30/14 Pct Recovery = 91% Analysis Date = 12/30/14 Pct Recovery = 91% Analysis Date = 12/21/14 Pct Recovery = 91% Analysis Date = 12/21/14 Pct Recovery = 91% Analysis Date = 12/11/14 Pct Recovery = 91% Analysis Date = 12/11/14 Pct Recovery = 91% Analysis Date = 12/02/14 Pct Recovery = 91% Analysis Date = 12/02/14 Pct Recovery = 91% Analysis Date = 11/22/14 Pct Recovery = 91% Analysis Date = 11/22/14 Pct Recovery = 91% Analysis Date = 11/13/14 Pct Recovery = 91% Analysis Date = 11/13/14 Pct Recovery = 91% Analysis Date = 11/04/14 Pct Recovery = 91% Analysis Date = 11/04/14 Pct Recovery = 91% Analysis Date = 10/25/14 Pct Recovery = 91% Analysis Date = 10/25/14 Pct Recovery = 91% Analysis Date = 10/16/14 Pct Recovery = 91% Analysis Date = 10/16/14 Pct Recovery = 91% Analysis Date = 10/06/14 Pct Recovery = 91% Analysis Date = 10/06/14 Pct Recovery = 91% Analysis Date = 09/27/14 Pct Recovery = 91% Analysis Date = 09/27/14 Pct Recovery = 91% Analysis Date = 09/18/14 Pct Recovery = 92% Analysis Date = 09/18/14 Pct Recovery = 92% Analysis Date = 09/08/14 Pct Recovery = 92% Analysis Date = 09/08/14 Pct Recovery = 92% Analysis Date = 08/30/14 Pct Recovery = 92% Analysis Date = 08/30/14 Pct Recovery = 92% Analysis Date = 08/20/14 Pct Recovery = 92% Analysis Date = 08/20/14 Pct Recovery = 92% Analysis Date = 08/11/14 Pct Recovery = 92% Analysis Date = 08/11/14 Pct Recovery = 92% Analysis Date = 08/02/14 Pct Recovery = 92% Analysis Date = 08/02/14 Pct Recovery = 92% Analysis Date = 07/23/14 Pct Recovery = 92% Analysis Date = 07/23/14 Pct Recovery = 92% Analysis Date = 07/14/14 Pct Recovery = 92% Analysis Date = 07/14/14 Pct Recovery = 92% Analysis Date = 07/04/14 Pct Recovery = 92% Analysis Date = 07/04/14 Pct Recovery = 92% Analysis Date = 06/25/14 Pct Recovery = 92% Analysis Date = 06/25/14 Pct Recovery = 92% Analysis Date = 06/16/14 Pct Recovery = 92% Analysis Date = 06/16/14 Pct Recovery = 92% Analysis Date = 06/06/14 Pct Recovery = 92% Analysis Date = 06/06/14 Pct Recovery = 92% Analysis Date = 05/28/14 Pct Recovery = 92% Analysis Date = 05/28/14 Pct Recovery = 92% Analysis Date = 05/18/14 Pct Recovery = 92% Analysis Date = 05/18/14 Pct Recovery = 92% Analysis Date = 05/09/14 Pct Recovery = 93% Analysis Date = 05/09/14 Pct Recovery = 93% Analysis Date = 04/30/14 Pct Recovery = 93% Analysis Date = 04/30/14 Pct Recovery = 93% Analysis Date = 04/20/14 Pct Recovery = 93% Analysis Date = 04/20/14 Pct Recovery = 93% Analysis Date = 04/11/14 Pct Recovery = 93% Analysis Date = 04/11/14 Pct Recovery = 93% Analysis Date = 04/01/14 Pct Recovery = 94% Analysis Date = 04/01/14 Pct Recovery = 94% Analysis Date = 03/23/14 Pct Recovery = 94% Analysis Date = 03/23/14 Pct Recovery = 94% Analysis Date = 03/14/14 Pct Recovery = 94% Analysis Date = 03/14/14 Pct Recovery = 94% Analysis Date = 03/04/14 Pct Recovery = 94% Analysis Date = 03/04/14 Pct Recovery = 94% Analysis Date = 02/23/14 Pct Recovery = 95% Analysis Date = 02/23/14 Pct Recovery = 95% Analysis Date = 02/13/14 Pct Recovery = 95% Analysis Date = 02/13/14 Pct Recovery = 95% Analysis Date = 02/04/14 Pct Recovery = 95% Analysis Date = 02/04/14 Pct Recovery = 95% Analysis Date = 01/26/14 Pct Recovery = 95% Analysis Date = 01/26/14 Pct Recovery = 95% Analysis Date = 01/16/14 Pct Recovery = 96% Analysis Date = 01/16/14 Pct Recovery = 96% Analysis Date = 01/07/14 Pct Recovery = 96% Analysis Date = 01/07/14 Pct Recovery = 96% Analysis Date = 12/28/13 Pct Recovery = 96% Analysis Date = 12/28/13 Pct Recovery = 96% Analysis Date = 12/19/13 Pct Recovery = 96% Analysis Date = 12/19/13 Pct Recovery = 96% Analysis Date = 12/10/13 Pct Recovery = 96% Analysis Date = 12/10/13 Pct Recovery = 96% Analysis Date = 11/30/13 Pct Recovery = 96% Analysis Date = 11/30/13 Pct Recovery = 96% Analysis Date = 11/21/13 Pct Recovery = 97% Analysis Date = 11/21/13 Pct Recovery = 97% Analysis Date = 11/11/13 Pct Recovery = 97% Analysis Date = 11/11/13 Pct Recovery = 97% Analysis Date = 11/02/13 Pct Recovery = 97% Analysis Date = 11/02/13 Pct Recovery = 97% Analysis Date = 10/24/13 Pct Recovery = 97% Analysis Date = 10/24/13 Pct Recovery = 97% Analysis Date = 10/14/13 Pct Recovery = 97% Analysis Date = 10/14/13 Pct Recovery = 97% Analysis Date = 10/05/13 Pct Recovery = 97% Analysis Date = 10/05/13 Pct Recovery = 97% Analysis Date = 09/25/13 Pct Recovery = 97% Analysis Date = 09/25/13 Pct Recovery = 97% Analysis Date = 09/16/13 Pct Recovery = 97% Analysis Date = 09/16/13 Pct Recovery = 97% Analysis Date = 09/07/13 Pct Recovery = 98% Analysis Date = 09/07/13 Pct Recovery = 98% Analysis Date = 08/28/13 Pct Recovery = 98% Analysis Date = 08/28/13 Pct Recovery = 98% Analysis Date = 08/19/13 Pct Recovery = 98% Analysis Date = 08/19/13 Pct Recovery = 98% Analysis Date = 08/09/13 Pct Recovery = 98% Analysis Date = 08/09/13 Pct Recovery = 98% Analysis Date = 07/31/13 Pct Recovery = 98% Analysis Date = 07/31/13 Pct Recovery = 98% Analysis Date = 07/22/13 Pct Recovery = 98% Analysis Date = 07/22/13 Pct Recovery = 98% Analysis Date = 07/12/13 Pct Recovery = 98% Analysis Date = 07/12/13 Pct Recovery = 98% Analysis Date = 07/03/13 Pct Recovery = 98% Analysis Date = 07/03/13 Pct Recovery = 98% Analysis Date = 06/23/13 Pct Recovery = 98% Analysis Date = 06/23/13 Pct Recovery = 98% Analysis Date = 06/14/13 Pct Recovery = 99% Analysis Date = 06/14/13 Pct Recovery = 99% Analysis Date = 06/05/13 Pct Recovery = 99% Analysis Date = 06/05/13 Pct Recovery = 99% Analysis Date = 05/26/13 Pct Recovery = 99% Analysis Date = 05/26/13 Pct Recovery = 99% Analysis Date = 05/17/13 Pct Recovery = 99% Analysis Date = 05/17/13 Pct Recovery = 99% Analysis Date = 05/07/13 Pct Recovery = 99% Analysis Date = 05/07/13 Pct Recovery = 99% Analysis Date = 04/28/13 Pct Recovery = 99% Analysis Date = 04/28/13 Pct Recovery = 99% Analysis Date = 04/19/13 Pct Recovery = 99% Analysis Date = 04/19/13 Pct Recovery = 99% Analysis Date = 04/09/13 Pct Recovery = 99% Analysis Date = 04/09/13 Pct Recovery = 99% Analysis Date = 03/31/13 Pct Recovery = 99% Analysis Date = 03/31/13 Pct Recovery = 99% Analysis Date = 03/21/13 Pct Recovery = 100% Analysis Date = 03/21/13 Pct Recovery = 100% Analysis Date = 03/12/13 Pct Recovery = 100% Analysis Date = 03/12/13 Pct Recovery = 100% Analysis Date = 03/03/13 Pct Recovery = 100% Analysis Date = 03/03/13 Pct Recovery = 100% Analysis Date = 02/21/13 Pct Recovery = 100% Analysis Date = 02/21/13 Pct Recovery = 100% Analysis Date = 02/12/13 Pct Recovery = 100% Analysis Date = 02/12/13 Pct Recovery = 100% Analysis Date = 02/02/13 Pct Recovery = 100% Analysis Date = 02/02/13 Pct Recovery = 100% Analysis Date = 01/24/13 Pct Recovery = 100% Analysis Date = 01/24/13 Pct Recovery = 100% Analysis Date = 01/15/13 Pct Recovery = 100% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
ALACHLOR

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 78 94% 16% 92% 14%
Total 78 94% 16% 92% 14%

Sample Statistics
ALACHLOR

Characteristic N % % Basis
Plotted 78 99% Spiked
Estimated Values 1 1% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 79 .  
False Negatives 1 1% 1 out of 79
Not Spiked 39 .  
False Positives 0 0% 0 out of 39

OBSP Determination:
ALPHA-ENDOSULFAN (ENDOSULFAN I)
METHOD: 2033 , TESTIDCODE: 34362GCM39

Laboratory ID = 20130250061 Lab Value = 0.252 Expected Conc. = 0.3 Report level label = 0.006 Pct Recovery = 84% Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl SpecificMix = A088380 Laboratory ID = 20140230082 Lab Value = 0.133 Expected Conc. = 0.15 Report level label = 0.006 Pct Recovery = 89% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl SpecificMix = A093651 Laboratory ID = 20132420001 Lab Value = 0.130 Expected Conc. = 0.15 Report level label = 0.006 Pct Recovery = 87% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl SpecificMix = A093651 Laboratory ID = 20130810108 Lab Value = 0.121 Expected Conc. = 0.15 Report level label = 0.006 Pct Recovery = 81% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl SpecificMix = T1120530013 Laboratory ID = 20123560092 Lab Value = 0.120 Expected Conc. = 0.15 Report level label = 0.006 Pct Recovery = 80% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = T1120530013 Laboratory ID = 20172510330 Lab Value = 0.055 Expected Conc. = 0.067 Report level label = 0.01 Pct Recovery = 82% Analysis Date = 12/29/17 SpikeMix = ChemService 6537100: 100 µl & Abs 071817Pest: 100 µl SpecificMix = 6537100 Laboratory ID = 20161880109 Lab Value = 0.068 Expected Conc. = 0.063 Report level label = 0.01 Pct Recovery = 108% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl SpecificMix = 03FF076 Laboratory ID = 20163370001 Lab Value = 0.068 Expected Conc. = 0.0625 Report level label = 0.01 Pct Recovery = 109% Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl SpecificMix = B20160331 Laboratory ID = 20163150006 Lab Value = 0.045 Expected Conc. = 0.0625 Report level label = 0.01 Pct Recovery = 72% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl SpecificMix = B20160331 Laboratory ID = 20140860102 Lab Value = 0.043 Expected Conc. = 0.06 Report level label = 0.006 Pct Recovery = 72% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl SpecificMix = A093651 Laboratory ID = 20133400002 Lab Value = 0.060 Expected Conc. = 0.06 Report level label = 0.006 Pct Recovery = 100% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = A093651 Laboratory ID = 20132910008 Lab Value = 0.048 Expected Conc. = 0.06 Report level label = 0.006 Pct Recovery = 80% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = A093651 Laboratory ID = 20131920149 Lab Value = 0.059 Expected Conc. = 0.06 Report level label = 0.006 Pct Recovery = 98% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl SpecificMix = A093651 Laboratory ID = 20131230084 Lab Value = 0.052 Expected Conc. = 0.06 Report level label = 0.006 Pct Recovery = 86% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl SpecificMix = A088380 Laboratory ID = 20130650005 Lab Value = 0.040 Expected Conc. = 0.06 Report level label = 0.006 Pct Recovery = 67% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl SpecificMix = A088380 Laboratory ID = 20130390105 Lab Value = 0.041 Expected Conc. = 0.06 Report level label = 0.006 Pct Recovery = 68% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl SpecificMix = T1120530013 Laboratory ID = 20172020035 Lab Value = 0.052 Expected Conc. = 0.052 Report level label = 0.01 Pct Recovery = 101% Analysis Date = 11/07/17 SpikeMix = Abs 071717Pest: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20170960001 Lab Value = 0.040 Expected Conc. = 0.0504 Report level label = 0.01 Pct Recovery = 78% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl SpecificMix = 03FF076 Laboratory ID = 20171720140 Lab Value = 0.053 Expected Conc. = 0.05 Report level label = 0.01 Pct Recovery = 107% Analysis Date = 08/31/17 SpikeMix = Supelco LC20138V: 80 µl & Phenova B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20171660002 Lab Value = 0.050 Expected Conc. = 0.05 Report level label = 0.01 Pct Recovery = 99% Analysis Date = 08/23/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20170190026 Lab Value = 0.042 Expected Conc. = 0.05 Report level label = 0.01 Pct Recovery = 85% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20161470001 Lab Value = 0.033 Expected Conc. = 0.05 Report level label = 0.01 Pct Recovery = 66% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20140100085 Lab Value = 0.033 Expected Conc. = 0.04 Report level label = 0.006 Pct Recovery = 83% Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl SpecificMix = T1130514013 Laboratory ID = 20132490342 Lab Value = 0.039 Expected Conc. = 0.04 Report level label = 0.006 Pct Recovery = 97% Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl SpecificMix = T1130514013 Laboratory ID = 20152750006 Lab Value = 0.024 Expected Conc. = 0.036 Report level label = 0.01 Pct Recovery = 68% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl SpecificMix = 040615 Laboratory ID = 20152610011 Lab Value = 0.041 Expected Conc. = 0.036 Report level label = 0.006 Pct Recovery = 115% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl SpecificMix = 040615 Laboratory ID = 20172370001 Lab Value = 0.033 Expected Conc. = 0.0335 Report level label = 0.01 Pct Recovery = 98% Analysis Date = 11/18/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6537100: 50 µl SpecificMix = 6537100 Laboratory ID = 20172230001 Lab Value = 0.034 Expected Conc. = 0.0335 Report level label = 0.01 Pct Recovery = 103% Analysis Date = 10/19/17 SpikeMix = ChemService 6472100: 50 µl & Abs 071717Pest: 50 µl SpecificMix = 071717Pest Laboratory ID = 20171510080 Lab Value = 0.027 Expected Conc. = 0.0252 Report level label = 0.01 Pct Recovery = 105% Analysis Date = 06/09/17 SpikeMix = Supelco LC20138V: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20170460061 Lab Value = 0.022 Expected Conc. = 0.0252 Report level label = 0.01 Pct Recovery = 89% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl SpecificMix = 03FF076 Laboratory ID = 20162660005 Lab Value = 0.024 Expected Conc. = 0.0252 Report level label = 0.01 Pct Recovery = 97% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl SpecificMix = 03FF076 Laboratory ID = 20161600087 Lab Value = 0.020 Expected Conc. = 0.0252 Report level label = 0.01 Pct Recovery = 79% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20161340228 Lab Value = 0.021 Expected Conc. = 0.0252 Report level label = 0.01 Pct Recovery = 81% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl SpecificMix = 03FF076 Laboratory ID = 20161190075 Lab Value = 0.023 Expected Conc. = 0.0252 Report level label = 0.01 Pct Recovery = 90% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20171160110 Lab Value = 0.025 Expected Conc. = 0.025 Report level label = 0.01 Pct Recovery = 99% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = B20160331 Laboratory ID = 20162380004 Lab Value = 0.022 Expected Conc. = 0.025 Report level label = 0.01 Pct Recovery = 88% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = B20160331 Laboratory ID = 20162150213 Lab Value = 0.027 Expected Conc. = 0.025 Report level label = 0.01 Pct Recovery = 108% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl SpecificMix = B20160331 Laboratory ID = 20150720069 Lab Value = 0.025 Expected Conc. = 0.024 Report level label = 0.006 Pct Recovery = 105% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 03DD006 Laboratory ID = 20143110108 Lab Value = 0.021 Expected Conc. = 0.024 Report level label = 0.006 Pct Recovery = 85% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 03DD006 Laboratory ID = 20142960086 Lab Value = 0.021 Expected Conc. = 0.024 Report level label = 0.006 Pct Recovery = 86% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 03DD006 Laboratory ID = 20142270001 Lab Value = 0.022 Expected Conc. = 0.024 Report level label = 0.006 Pct Recovery = 90% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl SpecificMix = 03DD006 Laboratory ID = 20142720002 Lab Value = 0.023 Expected Conc. = 0.0239 Report level label = 0.006 Pct Recovery = 97% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl SpecificMix = LC06435 Laboratory ID = 20142530087 Lab Value = 0.019 Expected Conc. = 0.0239 Report level label = 0.006 Pct Recovery = 79% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl SpecificMix = LC06435 Laboratory ID = 20141570088 Lab Value = 0.012 Expected Conc. = 0.0239 Report level label = 0.006 Pct Recovery = 51% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl SpecificMix = LC06435 Laboratory ID = 20141220025 Lab Value = 0.021 Expected Conc. = 0.0239 Report level label = 0.006 Pct Recovery = 87% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl SpecificMix = LC06435 Laboratory ID = 20131370001 Lab Value = 0.024 Expected Conc. = 0.0225 Report level label = 0.006 Pct Recovery = 107% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl SpecificMix = 1473000 Laboratory ID = 20173120093 Lab Value = 0.018 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 90% Analysis Date = 03/10/18 SpikeMix = ChemService 6472100: 30 µl & ChemService 6537100: 30 µl SpecificMix = 6537100 Laboratory ID = 20172780018 Lab Value = 0.022 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 107% Analysis Date = 02/08/18 SpikeMix = ChemService 6537100: 30 µl & Abs 071817Pest: 30 µl SpecificMix = 6537100 Laboratory ID = 20140370077 Lab Value = 0.019 Expected Conc. = 0.02 Report level label = 0.006 Pct Recovery = 94% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl SpecificMix = T1130514013 Laboratory ID = 20132690010 Lab Value = 0.016 Expected Conc. = 0.02 Report level label = 0.006 Pct Recovery = 82% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl SpecificMix = T1130514013 Laboratory ID = 20161260151 Lab Value = 0.016 Expected Conc. = 0.018 Report level label = 0.01 Pct Recovery = 87% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = EN150513008 Laboratory ID = 20160770090 Lab Value = 0.014 Expected Conc. = 0.018 Report level label = 0.01 Pct Recovery = 79% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = EN150513008 Laboratory ID = 20153510109 Lab Value = 0.014 Expected Conc. = 0.018 Report level label = 0.01 Pct Recovery = 77% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = EN150513008 Laboratory ID = 20152330039 Lab Value = 0.015 Expected Conc. = 0.018 Report level label = 0.006 Pct Recovery = 83% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl SpecificMix = EN150513008 Laboratory ID = 20151900132 Lab Value = 0.012 Expected Conc. = 0.018 Report level label = 0.006 Pct Recovery = 64% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl SpecificMix = 040615 Laboratory ID = 20151550293 Lab Value = 0.016 Expected Conc. = 0.018 Report level label = 0.006 Pct Recovery = 91% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl SpecificMix = 040615 Laboratory ID = 20142200164 Lab Value = 0.012 Expected Conc. = 0.012 Report level label = 0.006 Pct Recovery = 100% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 03DD006 Laboratory ID = 20141640076 Lab Value = 0.008 Expected Conc. = 0.012 Report level label = 0.006 Pct Recovery = 64% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = 03DD006 Laboratory ID = 20141420140 Lab Value = 0.016 Expected Conc. = 0.012 Report level label = 0.006 Pct Recovery = 130% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 03DD006 Laboratory ID = 20141080004 Lab Value = 0.010 Expected Conc. = 0.012 Report level label = 0.006 Pct Recovery = 81% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl SpecificMix = 03DD006 Laboratory ID = 20150150115 Lab Value = 0.011 Expected Conc. = 0.012 Report level label = 0.006 Pct Recovery = 92% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl SpecificMix = LC06435 Laboratory ID = 20143370094 Lab Value = 0.012 Expected Conc. = 0.012 Report level label = 0.006 Pct Recovery = 97% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl SpecificMix = LC06435 Laboratory ID = 20141910243 Lab Value = 0.012 Expected Conc. = 0.012 Report level label = 0.006 Pct Recovery = 96% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = LC06435 Laboratory ID = 20141840097 Lab Value = 0.010 Expected Conc. = 0.012 Report level label = 0.006 Pct Recovery = 84% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl SpecificMix = LC06435 Laboratory ID = 20152190003 Lab Value = 0.008 Expected Conc. = 0.009 Report level label = 0.006 Pct Recovery = 86% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150513008 Laboratory ID = 20151480170 Lab Value = 0.007 Expected Conc. = 0.009 Report level label = 0.006 Pct Recovery = 74% Analysis Date = 06/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150513008 Laboratory ID = 20151380009 Lab Value = 0.004 Expected Conc. = 0.009 Report level label = 0.006 Pct Recovery = 47% Analysis Date = 05/30/15 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Laboratory ID = 20151210037 Lab Value = 0.007 Expected Conc. = 0.009 Report level label = 0.006 Pct Recovery = 74% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Laboratory ID = 20140730138 Lab Value = 0.008 Expected Conc. = 0.009 Report level label = 0.006 Pct Recovery = 90% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 1473000 Laboratory ID = 20133470008 Lab Value = 0.008 Expected Conc. = 0.009 Report level label = 0.006 Pct Recovery = 84% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl SpecificMix = 1473000 Laboratory ID = 20133310030 Lab Value = 0.011 Expected Conc. = 0.009 Report level label = 0.006 Pct Recovery = 126% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl SpecificMix = 1473000 Laboratory ID = 20131790009 Lab Value = 0.010 Expected Conc. = 0.009 Report level label = 0.006 Pct Recovery = 106% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl SpecificMix = 1473000 Laboratory ID = 20131650073 Lab Value = 0.008 Expected Conc. = 0.009 Report level label = 0.006 Pct Recovery = 90% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl SpecificMix = 1473000 Laboratory ID = 20133050050 Lab Value = 0.009 Expected Conc. = 0.008 Report level label = 0.006 Pct Recovery = 110% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl SpecificMix = T1130514013 Laboratory ID = 20132280016 Lab Value = 0.008 Expected Conc. = 0.008 Report level label = 0.006 Pct Recovery = 101% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl SpecificMix = T1130514013 Laboratory ID = 20161050143 Lab Value = 0.008 Expected Conc. = 0.009 Report level label = 0.01 Pct Recovery = 90% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Laboratory ID = 20160430111 Lab Value = 0.009 Expected Conc. = 0.009 Report level label = 0.01 Pct Recovery = 101% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Laboratory ID = 20160560044 Lab Value = 0.009 Expected Conc. = 0.009 Report level label = 0.01 Pct Recovery = 94% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl SpecificMix = EN150513008 Laboratory ID = 20160070059 Lab Value = 0.008 Expected Conc. = 0.009 Report level label = 0.01 Pct Recovery = 89% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = 040615 Laboratory ID = 20153160001 Lab Value = 0.008 Expected Conc. = 0.009 Report level label = 0.01 Pct Recovery = 92% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = EN150513008 Laboratory ID = 20153030068 Lab Value = 0.009 Expected Conc. = 0.009 Report level label = 0.01 Pct Recovery = 102% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150513008 Analysis Date = 03/10/18 Pct Recovery = 99% Analysis Date = 02/28/18 Pct Recovery = 99% Analysis Date = 02/28/18 Pct Recovery = 99% Analysis Date = 02/19/18 Pct Recovery = 98% Analysis Date = 02/19/18 Pct Recovery = 98% Analysis Date = 02/09/18 Pct Recovery = 98% Analysis Date = 02/09/18 Pct Recovery = 98% Analysis Date = 01/31/18 Pct Recovery = 98% Analysis Date = 01/31/18 Pct Recovery = 98% Analysis Date = 01/22/18 Pct Recovery = 98% Analysis Date = 01/22/18 Pct Recovery = 98% Analysis Date = 01/12/18 Pct Recovery = 98% Analysis Date = 01/12/18 Pct Recovery = 98% Analysis Date = 01/03/18 Pct Recovery = 98% Analysis Date = 01/03/18 Pct Recovery = 98% Analysis Date = 12/24/17 Pct Recovery = 98% Analysis Date = 12/24/17 Pct Recovery = 98% Analysis Date = 12/15/17 Pct Recovery = 97% Analysis Date = 12/15/17 Pct Recovery = 97% Analysis Date = 12/06/17 Pct Recovery = 97% Analysis Date = 12/06/17 Pct Recovery = 97% Analysis Date = 11/26/17 Pct Recovery = 97% Analysis Date = 11/26/17 Pct Recovery = 97% Analysis Date = 11/17/17 Pct Recovery = 97% Analysis Date = 11/17/17 Pct Recovery = 97% Analysis Date = 11/07/17 Pct Recovery = 97% Analysis Date = 11/07/17 Pct Recovery = 97% Analysis Date = 10/29/17 Pct Recovery = 97% Analysis Date = 10/29/17 Pct Recovery = 97% Analysis Date = 10/20/17 Pct Recovery = 96% Analysis Date = 10/20/17 Pct Recovery = 96% Analysis Date = 10/10/17 Pct Recovery = 96% Analysis Date = 10/10/17 Pct Recovery = 96% Analysis Date = 10/01/17 Pct Recovery = 96% Analysis Date = 10/01/17 Pct Recovery = 96% Analysis Date = 09/21/17 Pct Recovery = 96% Analysis Date = 09/21/17 Pct Recovery = 96% Analysis Date = 09/12/17 Pct Recovery = 96% Analysis Date = 09/12/17 Pct Recovery = 96% Analysis Date = 09/03/17 Pct Recovery = 96% Analysis Date = 09/03/17 Pct Recovery = 96% Analysis Date = 08/24/17 Pct Recovery = 96% Analysis Date = 08/24/17 Pct Recovery = 96% Analysis Date = 08/15/17 Pct Recovery = 95% Analysis Date = 08/15/17 Pct Recovery = 95% Analysis Date = 08/05/17 Pct Recovery = 95% Analysis Date = 08/05/17 Pct Recovery = 95% Analysis Date = 07/27/17 Pct Recovery = 95% Analysis Date = 07/27/17 Pct Recovery = 95% Analysis Date = 07/18/17 Pct Recovery = 95% Analysis Date = 07/18/17 Pct Recovery = 95% Analysis Date = 07/08/17 Pct Recovery = 95% Analysis Date = 07/08/17 Pct Recovery = 95% Analysis Date = 06/29/17 Pct Recovery = 95% Analysis Date = 06/29/17 Pct Recovery = 95% Analysis Date = 06/19/17 Pct Recovery = 95% Analysis Date = 06/19/17 Pct Recovery = 95% Analysis Date = 06/10/17 Pct Recovery = 94% Analysis Date = 06/10/17 Pct Recovery = 94% Analysis Date = 06/01/17 Pct Recovery = 94% Analysis Date = 06/01/17 Pct Recovery = 94% Analysis Date = 05/22/17 Pct Recovery = 94% Analysis Date = 05/22/17 Pct Recovery = 94% Analysis Date = 05/13/17 Pct Recovery = 94% Analysis Date = 05/13/17 Pct Recovery = 94% Analysis Date = 05/03/17 Pct Recovery = 94% Analysis Date = 05/03/17 Pct Recovery = 94% Analysis Date = 04/24/17 Pct Recovery = 94% Analysis Date = 04/24/17 Pct Recovery = 94% Analysis Date = 04/15/17 Pct Recovery = 94% Analysis Date = 04/15/17 Pct Recovery = 94% Analysis Date = 04/05/17 Pct Recovery = 93% Analysis Date = 04/05/17 Pct Recovery = 93% Analysis Date = 03/27/17 Pct Recovery = 93% Analysis Date = 03/27/17 Pct Recovery = 93% Analysis Date = 03/17/17 Pct Recovery = 93% Analysis Date = 03/17/17 Pct Recovery = 93% Analysis Date = 03/08/17 Pct Recovery = 93% Analysis Date = 03/08/17 Pct Recovery = 93% Analysis Date = 02/27/17 Pct Recovery = 93% Analysis Date = 02/27/17 Pct Recovery = 93% Analysis Date = 02/17/17 Pct Recovery = 93% Analysis Date = 02/17/17 Pct Recovery = 93% Analysis Date = 02/08/17 Pct Recovery = 93% Analysis Date = 02/08/17 Pct Recovery = 93% Analysis Date = 01/29/17 Pct Recovery = 92% Analysis Date = 01/29/17 Pct Recovery = 92% Analysis Date = 01/20/17 Pct Recovery = 92% Analysis Date = 01/20/17 Pct Recovery = 92% Analysis Date = 01/11/17 Pct Recovery = 92% Analysis Date = 01/11/17 Pct Recovery = 92% Analysis Date = 01/01/17 Pct Recovery = 92% Analysis Date = 01/01/17 Pct Recovery = 92% Analysis Date = 12/23/16 Pct Recovery = 92% Analysis Date = 12/23/16 Pct Recovery = 92% Analysis Date = 12/13/16 Pct Recovery = 92% Analysis Date = 12/13/16 Pct Recovery = 92% Analysis Date = 12/04/16 Pct Recovery = 91% Analysis Date = 12/04/16 Pct Recovery = 91% Analysis Date = 11/25/16 Pct Recovery = 91% Analysis Date = 11/25/16 Pct Recovery = 91% Analysis Date = 11/15/16 Pct Recovery = 91% Analysis Date = 11/15/16 Pct Recovery = 91% Analysis Date = 11/06/16 Pct Recovery = 91% Analysis Date = 11/06/16 Pct Recovery = 91% Analysis Date = 10/27/16 Pct Recovery = 91% Analysis Date = 10/27/16 Pct Recovery = 91% Analysis Date = 10/18/16 Pct Recovery = 91% Analysis Date = 10/18/16 Pct Recovery = 91% Analysis Date = 10/09/16 Pct Recovery = 91% Analysis Date = 10/09/16 Pct Recovery = 91% Analysis Date = 09/29/16 Pct Recovery = 90% Analysis Date = 09/29/16 Pct Recovery = 90% Analysis Date = 09/20/16 Pct Recovery = 90% Analysis Date = 09/20/16 Pct Recovery = 90% Analysis Date = 09/10/16 Pct Recovery = 90% Analysis Date = 09/10/16 Pct Recovery = 90% Analysis Date = 09/01/16 Pct Recovery = 90% Analysis Date = 09/01/16 Pct Recovery = 90% Analysis Date = 08/23/16 Pct Recovery = 90% Analysis Date = 08/23/16 Pct Recovery = 90% Analysis Date = 08/13/16 Pct Recovery = 90% Analysis Date = 08/13/16 Pct Recovery = 90% Analysis Date = 08/04/16 Pct Recovery = 89% Analysis Date = 08/04/16 Pct Recovery = 89% Analysis Date = 07/25/16 Pct Recovery = 89% Analysis Date = 07/25/16 Pct Recovery = 89% Analysis Date = 07/16/16 Pct Recovery = 89% Analysis Date = 07/16/16 Pct Recovery = 89% Analysis Date = 07/07/16 Pct Recovery = 89% Analysis Date = 07/07/16 Pct Recovery = 89% Analysis Date = 06/27/16 Pct Recovery = 89% Analysis Date = 06/27/16 Pct Recovery = 89% Analysis Date = 06/18/16 Pct Recovery = 89% Analysis Date = 06/18/16 Pct Recovery = 89% Analysis Date = 06/08/16 Pct Recovery = 88% Analysis Date = 06/08/16 Pct Recovery = 88% Analysis Date = 05/30/16 Pct Recovery = 88% Analysis Date = 05/30/16 Pct Recovery = 88% Analysis Date = 05/21/16 Pct Recovery = 88% Analysis Date = 05/21/16 Pct Recovery = 88% Analysis Date = 05/11/16 Pct Recovery = 88% Analysis Date = 05/11/16 Pct Recovery = 88% Analysis Date = 05/02/16 Pct Recovery = 88% Analysis Date = 05/02/16 Pct Recovery = 88% Analysis Date = 04/22/16 Pct Recovery = 88% Analysis Date = 04/22/16 Pct Recovery = 88% Analysis Date = 04/13/16 Pct Recovery = 88% Analysis Date = 04/13/16 Pct Recovery = 88% Analysis Date = 04/04/16 Pct Recovery = 87% Analysis Date = 04/04/16 Pct Recovery = 87% Analysis Date = 03/25/16 Pct Recovery = 87% Analysis Date = 03/25/16 Pct Recovery = 87% Analysis Date = 03/16/16 Pct Recovery = 87% Analysis Date = 03/16/16 Pct Recovery = 87% Analysis Date = 03/06/16 Pct Recovery = 87% Analysis Date = 03/06/16 Pct Recovery = 87% Analysis Date = 02/26/16 Pct Recovery = 87% Analysis Date = 02/26/16 Pct Recovery = 87% Analysis Date = 02/17/16 Pct Recovery = 87% Analysis Date = 02/17/16 Pct Recovery = 87% Analysis Date = 02/07/16 Pct Recovery = 87% Analysis Date = 02/07/16 Pct Recovery = 87% Analysis Date = 01/29/16 Pct Recovery = 87% Analysis Date = 01/29/16 Pct Recovery = 87% Analysis Date = 01/19/16 Pct Recovery = 87% Analysis Date = 01/19/16 Pct Recovery = 87% Analysis Date = 01/10/16 Pct Recovery = 87% Analysis Date = 01/10/16 Pct Recovery = 87% Analysis Date = 01/01/16 Pct Recovery = 87% Analysis Date = 01/01/16 Pct Recovery = 87% Analysis Date = 12/22/15 Pct Recovery = 87% Analysis Date = 12/22/15 Pct Recovery = 87% Analysis Date = 12/13/15 Pct Recovery = 86% Analysis Date = 12/13/15 Pct Recovery = 86% Analysis Date = 12/03/15 Pct Recovery = 86% Analysis Date = 12/03/15 Pct Recovery = 86% Analysis Date = 11/24/15 Pct Recovery = 86% Analysis Date = 11/24/15 Pct Recovery = 86% Analysis Date = 11/15/15 Pct Recovery = 86% Analysis Date = 11/15/15 Pct Recovery = 86% Analysis Date = 11/05/15 Pct Recovery = 86% Analysis Date = 11/05/15 Pct Recovery = 86% Analysis Date = 10/27/15 Pct Recovery = 86% Analysis Date = 10/27/15 Pct Recovery = 86% Analysis Date = 10/17/15 Pct Recovery = 86% Analysis Date = 10/17/15 Pct Recovery = 86% Analysis Date = 10/08/15 Pct Recovery = 86% Analysis Date = 10/08/15 Pct Recovery = 86% Analysis Date = 09/29/15 Pct Recovery = 86% Analysis Date = 09/29/15 Pct Recovery = 86% Analysis Date = 09/19/15 Pct Recovery = 86% Analysis Date = 09/19/15 Pct Recovery = 86% Analysis Date = 09/10/15 Pct Recovery = 86% Analysis Date = 09/10/15 Pct Recovery = 86% Analysis Date = 08/31/15 Pct Recovery = 86% Analysis Date = 08/31/15 Pct Recovery = 86% Analysis Date = 08/22/15 Pct Recovery = 86% Analysis Date = 08/22/15 Pct Recovery = 86% Analysis Date = 08/13/15 Pct Recovery = 86% Analysis Date = 08/13/15 Pct Recovery = 86% Analysis Date = 08/03/15 Pct Recovery = 86% Analysis Date = 08/03/15 Pct Recovery = 86% Analysis Date = 07/25/15 Pct Recovery = 86% Analysis Date = 07/25/15 Pct Recovery = 86% Analysis Date = 07/15/15 Pct Recovery = 86% Analysis Date = 07/15/15 Pct Recovery = 86% Analysis Date = 07/06/15 Pct Recovery = 86% Analysis Date = 07/06/15 Pct Recovery = 86% Analysis Date = 06/27/15 Pct Recovery = 86% Analysis Date = 06/27/15 Pct Recovery = 86% Analysis Date = 06/17/15 Pct Recovery = 86% Analysis Date = 06/17/15 Pct Recovery = 86% Analysis Date = 06/08/15 Pct Recovery = 86% Analysis Date = 06/08/15 Pct Recovery = 86% Analysis Date = 05/29/15 Pct Recovery = 86% Analysis Date = 05/29/15 Pct Recovery = 86% Analysis Date = 05/20/15 Pct Recovery = 86% Analysis Date = 05/20/15 Pct Recovery = 86% Analysis Date = 05/11/15 Pct Recovery = 86% Analysis Date = 05/11/15 Pct Recovery = 86% Analysis Date = 05/01/15 Pct Recovery = 86% Analysis Date = 05/01/15 Pct Recovery = 86% Analysis Date = 04/22/15 Pct Recovery = 86% Analysis Date = 04/22/15 Pct Recovery = 86% Analysis Date = 04/12/15 Pct Recovery = 86% Analysis Date = 04/12/15 Pct Recovery = 86% Analysis Date = 04/03/15 Pct Recovery = 86% Analysis Date = 04/03/15 Pct Recovery = 86% Analysis Date = 03/25/15 Pct Recovery = 86% Analysis Date = 03/25/15 Pct Recovery = 86% Analysis Date = 03/15/15 Pct Recovery = 86% Analysis Date = 03/15/15 Pct Recovery = 86% Analysis Date = 03/06/15 Pct Recovery = 86% Analysis Date = 03/06/15 Pct Recovery = 86% Analysis Date = 02/24/15 Pct Recovery = 86% Analysis Date = 02/24/15 Pct Recovery = 86% Analysis Date = 02/15/15 Pct Recovery = 86% Analysis Date = 02/15/15 Pct Recovery = 86% Analysis Date = 02/06/15 Pct Recovery = 86% Analysis Date = 02/06/15 Pct Recovery = 86% Analysis Date = 01/27/15 Pct Recovery = 86% Analysis Date = 01/27/15 Pct Recovery = 86% Analysis Date = 01/18/15 Pct Recovery = 86% Analysis Date = 01/18/15 Pct Recovery = 86% Analysis Date = 01/08/15 Pct Recovery = 86% Analysis Date = 01/08/15 Pct Recovery = 86% Analysis Date = 12/30/14 Pct Recovery = 86% Analysis Date = 12/30/14 Pct Recovery = 86% Analysis Date = 12/21/14 Pct Recovery = 86% Analysis Date = 12/21/14 Pct Recovery = 86% Analysis Date = 12/11/14 Pct Recovery = 86% Analysis Date = 12/11/14 Pct Recovery = 86% Analysis Date = 12/02/14 Pct Recovery = 86% Analysis Date = 12/02/14 Pct Recovery = 86% Analysis Date = 11/22/14 Pct Recovery = 86% Analysis Date = 11/22/14 Pct Recovery = 86% Analysis Date = 11/13/14 Pct Recovery = 86% Analysis Date = 11/13/14 Pct Recovery = 86% Analysis Date = 11/04/14 Pct Recovery = 86% Analysis Date = 11/04/14 Pct Recovery = 86% Analysis Date = 10/25/14 Pct Recovery = 86% Analysis Date = 10/25/14 Pct Recovery = 86% Analysis Date = 10/16/14 Pct Recovery = 86% Analysis Date = 10/16/14 Pct Recovery = 86% Analysis Date = 10/06/14 Pct Recovery = 87% Analysis Date = 10/06/14 Pct Recovery = 87% Analysis Date = 09/27/14 Pct Recovery = 87% Analysis Date = 09/27/14 Pct Recovery = 87% Analysis Date = 09/18/14 Pct Recovery = 87% Analysis Date = 09/18/14 Pct Recovery = 87% Analysis Date = 09/08/14 Pct Recovery = 87% Analysis Date = 09/08/14 Pct Recovery = 87% Analysis Date = 08/30/14 Pct Recovery = 87% Analysis Date = 08/30/14 Pct Recovery = 87% Analysis Date = 08/20/14 Pct Recovery = 87% Analysis Date = 08/20/14 Pct Recovery = 87% Analysis Date = 08/11/14 Pct Recovery = 88% Analysis Date = 08/11/14 Pct Recovery = 88% Analysis Date = 08/02/14 Pct Recovery = 88% Analysis Date = 08/02/14 Pct Recovery = 88% Analysis Date = 07/23/14 Pct Recovery = 88% Analysis Date = 07/23/14 Pct Recovery = 88% Analysis Date = 07/14/14 Pct Recovery = 88% Analysis Date = 07/14/14 Pct Recovery = 88% Analysis Date = 07/04/14 Pct Recovery = 88% Analysis Date = 07/04/14 Pct Recovery = 88% Analysis Date = 06/25/14 Pct Recovery = 89% Analysis Date = 06/25/14 Pct Recovery = 89% Analysis Date = 06/16/14 Pct Recovery = 89% Analysis Date = 06/16/14 Pct Recovery = 89% Analysis Date = 06/06/14 Pct Recovery = 89% Analysis Date = 06/06/14 Pct Recovery = 89% Analysis Date = 05/28/14 Pct Recovery = 89% Analysis Date = 05/28/14 Pct Recovery = 89% Analysis Date = 05/18/14 Pct Recovery = 89% Analysis Date = 05/18/14 Pct Recovery = 89% Analysis Date = 05/09/14 Pct Recovery = 89% Analysis Date = 05/09/14 Pct Recovery = 89% Analysis Date = 04/30/14 Pct Recovery = 89% Analysis Date = 04/30/14 Pct Recovery = 89% Analysis Date = 04/20/14 Pct Recovery = 89% Analysis Date = 04/20/14 Pct Recovery = 89% Analysis Date = 04/11/14 Pct Recovery = 90% Analysis Date = 04/11/14 Pct Recovery = 90% Analysis Date = 04/01/14 Pct Recovery = 90% Analysis Date = 04/01/14 Pct Recovery = 90% Analysis Date = 03/23/14 Pct Recovery = 90% Analysis Date = 03/23/14 Pct Recovery = 90% Analysis Date = 03/14/14 Pct Recovery = 90% Analysis Date = 03/14/14 Pct Recovery = 90% Analysis Date = 03/04/14 Pct Recovery = 90% Analysis Date = 03/04/14 Pct Recovery = 90% Analysis Date = 02/23/14 Pct Recovery = 90% Analysis Date = 02/23/14 Pct Recovery = 90% Analysis Date = 02/13/14 Pct Recovery = 90% Analysis Date = 02/13/14 Pct Recovery = 90% Analysis Date = 02/04/14 Pct Recovery = 90% Analysis Date = 02/04/14 Pct Recovery = 90% Analysis Date = 01/26/14 Pct Recovery = 90% Analysis Date = 01/26/14 Pct Recovery = 90% Analysis Date = 01/16/14 Pct Recovery = 90% Analysis Date = 01/16/14 Pct Recovery = 90% Analysis Date = 01/07/14 Pct Recovery = 90% Analysis Date = 01/07/14 Pct Recovery = 90% Analysis Date = 12/28/13 Pct Recovery = 90% Analysis Date = 12/28/13 Pct Recovery = 90% Analysis Date = 12/19/13 Pct Recovery = 89% Analysis Date = 12/19/13 Pct Recovery = 89% Analysis Date = 12/10/13 Pct Recovery = 89% Analysis Date = 12/10/13 Pct Recovery = 89% Analysis Date = 11/30/13 Pct Recovery = 89% Analysis Date = 11/30/13 Pct Recovery = 89% Analysis Date = 11/21/13 Pct Recovery = 89% Analysis Date = 11/21/13 Pct Recovery = 89% Analysis Date = 11/11/13 Pct Recovery = 89% Analysis Date = 11/11/13 Pct Recovery = 89% Analysis Date = 11/02/13 Pct Recovery = 89% Analysis Date = 11/02/13 Pct Recovery = 89% Analysis Date = 10/24/13 Pct Recovery = 89% Analysis Date = 10/24/13 Pct Recovery = 89% Analysis Date = 10/14/13 Pct Recovery = 89% Analysis Date = 10/14/13 Pct Recovery = 89% Analysis Date = 10/05/13 Pct Recovery = 89% Analysis Date = 10/05/13 Pct Recovery = 89% Analysis Date = 09/25/13 Pct Recovery = 89% Analysis Date = 09/25/13 Pct Recovery = 89% Analysis Date = 09/16/13 Pct Recovery = 89% Analysis Date = 09/16/13 Pct Recovery = 89% Analysis Date = 09/07/13 Pct Recovery = 89% Analysis Date = 09/07/13 Pct Recovery = 89% Analysis Date = 08/28/13 Pct Recovery = 89% Analysis Date = 08/28/13 Pct Recovery = 89% Analysis Date = 08/19/13 Pct Recovery = 89% Analysis Date = 08/19/13 Pct Recovery = 89% Analysis Date = 08/09/13 Pct Recovery = 89% Analysis Date = 08/09/13 Pct Recovery = 89% Analysis Date = 07/31/13 Pct Recovery = 89% Analysis Date = 07/31/13 Pct Recovery = 89% Analysis Date = 07/22/13 Pct Recovery = 89% Analysis Date = 07/22/13 Pct Recovery = 89% Analysis Date = 07/12/13 Pct Recovery = 89% Analysis Date = 07/12/13 Pct Recovery = 89% Analysis Date = 07/03/13 Pct Recovery = 89% Analysis Date = 07/03/13 Pct Recovery = 89% Analysis Date = 06/23/13 Pct Recovery = 89% Analysis Date = 06/23/13 Pct Recovery = 89% Analysis Date = 06/14/13 Pct Recovery = 88% Analysis Date = 06/14/13 Pct Recovery = 88% Analysis Date = 06/05/13 Pct Recovery = 88% Analysis Date = 06/05/13 Pct Recovery = 88% Analysis Date = 05/26/13 Pct Recovery = 88% Analysis Date = 05/26/13 Pct Recovery = 88% Analysis Date = 05/17/13 Pct Recovery = 88% Analysis Date = 05/17/13 Pct Recovery = 88% Analysis Date = 05/07/13 Pct Recovery = 88% Analysis Date = 05/07/13 Pct Recovery = 88% Analysis Date = 04/28/13 Pct Recovery = 88% Analysis Date = 04/28/13 Pct Recovery = 88% Analysis Date = 04/19/13 Pct Recovery = 88% Analysis Date = 04/19/13 Pct Recovery = 88% Analysis Date = 04/09/13 Pct Recovery = 88% Analysis Date = 04/09/13 Pct Recovery = 88% Analysis Date = 03/31/13 Pct Recovery = 88% Analysis Date = 03/31/13 Pct Recovery = 88% Analysis Date = 03/21/13 Pct Recovery = 88% Analysis Date = 03/21/13 Pct Recovery = 88% Analysis Date = 03/12/13 Pct Recovery = 88% Analysis Date = 03/12/13 Pct Recovery = 88% Analysis Date = 03/03/13 Pct Recovery = 88% Analysis Date = 03/03/13 Pct Recovery = 88% Analysis Date = 02/21/13 Pct Recovery = 88% Analysis Date = 02/21/13 Pct Recovery = 88% Analysis Date = 02/12/13 Pct Recovery = 88% Analysis Date = 02/12/13 Pct Recovery = 88% Analysis Date = 02/02/13 Pct Recovery = 88% Analysis Date = 02/02/13 Pct Recovery = 88% Analysis Date = 01/24/13 Pct Recovery = 87% Analysis Date = 01/24/13 Pct Recovery = 87% Analysis Date = 01/15/13 Pct Recovery = 87% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
ALPHA-ENDOSULFAN (ENDOSULFAN I)

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 6 95% 6% 93% 8%
>= Reporting Level 75 89% 15% 88% 14%
Total 81 89% 15% 89% 14%

Sample Statistics
ALPHA-ENDOSULFAN (ENDOSULFAN I)

Characteristic N % % Basis
Plotted 81 100% Spiked
Estimated Values 2 2% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 81 .  
False Negatives 0 0% 0 out of 81
Not Spiked 37 .  
False Positives 0 0% 0 out of 37

OBSP Determination:
ATRAZINE
METHOD: 2033 , TESTIDCODE: 39632GCM35

Laboratory ID = 20130250061 Lab Value = 0.585 Expected Conc. = 0.6 Report level label = 0.008 Pct Recovery = 98% Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl SpecificMix = A088380 Laboratory ID = 20130810108 Lab Value = 0.280 Expected Conc. = 0.3005 Report level label = 0.008 Pct Recovery = 93% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl SpecificMix = T1120530013 Laboratory ID = 20123560092 Lab Value = 0.292 Expected Conc. = 0.3005 Report level label = 0.008 Pct Recovery = 97% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = T1120530013 Laboratory ID = 20140230082 Lab Value = 0.269 Expected Conc. = 0.3 Report level label = 0.008 Pct Recovery = 90% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl SpecificMix = A093651 Laboratory ID = 20132420001 Lab Value = 0.285 Expected Conc. = 0.3 Report level label = 0.008 Pct Recovery = 95% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl SpecificMix = A093651 Laboratory ID = 20140100085 Lab Value = 0.271 Expected Conc. = 0.25 Report level label = 0.008 Pct Recovery = 108% Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl SpecificMix = T1130514013 Laboratory ID = 20132490342 Lab Value = 0.271 Expected Conc. = 0.25 Report level label = 0.008 Pct Recovery = 108% Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl SpecificMix = T1130514013 Laboratory ID = 20140370077 Lab Value = 0.109 Expected Conc. = 0.125 Report level label = 0.008 Pct Recovery = 87% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl SpecificMix = T1130514013 Laboratory ID = 20132690010 Lab Value = 0.155 Expected Conc. = 0.125 Report level label = 0.008 Pct Recovery = 124% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl SpecificMix = T1130514013 Laboratory ID = 20131370001 Lab Value = 0.145 Expected Conc. = 0.1245 Report level label = 0.008 Pct Recovery = 116% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl SpecificMix = 1473000 Laboratory ID = 20130390105 Lab Value = 0.081 Expected Conc. = 0.1202 Report level label = 0.008 Pct Recovery = 67% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl SpecificMix = T1120530013 Laboratory ID = 20140860102 Lab Value = 0.087 Expected Conc. = 0.12 Report level label = 0.008 Pct Recovery = 73% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl SpecificMix = A093651 Laboratory ID = 20133400002 Lab Value = 0.120 Expected Conc. = 0.12 Report level label = 0.008 Pct Recovery = 100% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = A093651 Laboratory ID = 20132910008 Lab Value = 0.100 Expected Conc. = 0.12 Report level label = 0.008 Pct Recovery = 83% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = A093651 Laboratory ID = 20131920149 Lab Value = 0.115 Expected Conc. = 0.12 Report level label = 0.008 Pct Recovery = 96% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl SpecificMix = A093651 Laboratory ID = 20131230084 Lab Value = 0.136 Expected Conc. = 0.12 Report level label = 0.008 Pct Recovery = 113% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl SpecificMix = A088380 Laboratory ID = 20130650005 Lab Value = 0.082 Expected Conc. = 0.12 Report level label = 0.008 Pct Recovery = 68% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl SpecificMix = A088380 Laboratory ID = 20180390003 Lab Value = 0.057 Expected Conc. = 0.053 Report level label = 0.008 Pct Recovery = 108% Analysis Date = 04/06/18 SpikeMix = Spex Organics EN170808006: 100 µl & Abs 071717Pest: 100 µl SpecificMix = 071717Pest Laboratory ID = 20172510330 Lab Value = 0.052 Expected Conc. = 0.053 Report level label = 0.008 Pct Recovery = 98% Analysis Date = 12/29/17 SpikeMix = ChemService 6537100: 100 µl & Abs 071817Pest: 100 µl SpecificMix = 6537100 Laboratory ID = 20162860079 Lab Value = 0.059 Expected Conc. = 0.05 Report level label = 0.008 Pct Recovery = 118% Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl SpecificMix = 060916 Laboratory ID = 20163150006 Lab Value = 0.051 Expected Conc. = 0.05 Report level label = 0.008 Pct Recovery = 102% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl SpecificMix = 060916 Laboratory ID = 20133050050 Lab Value = 0.050 Expected Conc. = 0.05 Report level label = 0.008 Pct Recovery = 99% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl SpecificMix = T1130514013 Laboratory ID = 20132280016 Lab Value = 0.051 Expected Conc. = 0.05 Report level label = 0.008 Pct Recovery = 102% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl SpecificMix = T1130514013 Laboratory ID = 20140730138 Lab Value = 0.039 Expected Conc. = 0.0498 Report level label = 0.008 Pct Recovery = 78% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 1473000 Laboratory ID = 20133470008 Lab Value = 0.050 Expected Conc. = 0.0498 Report level label = 0.008 Pct Recovery = 101% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl SpecificMix = 1473000 Laboratory ID = 20133310030 Lab Value = 0.042 Expected Conc. = 0.0498 Report level label = 0.008 Pct Recovery = 84% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl SpecificMix = 1473000 Laboratory ID = 20131790009 Lab Value = 0.053 Expected Conc. = 0.0498 Report level label = 0.008 Pct Recovery = 107% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl SpecificMix = 1473000 Laboratory ID = 20131650073 Lab Value = 0.058 Expected Conc. = 0.0498 Report level label = 0.008 Pct Recovery = 116% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl SpecificMix = 1473000 Laboratory ID = 20152610011 Lab Value = 0.039 Expected Conc. = 0.0484 Report level label = 0.008 Pct Recovery = 80% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl SpecificMix = 0406-15-01 Laboratory ID = 20152460215 Lab Value = 0.045 Expected Conc. = 0.0484 Report level label = 0.008 Pct Recovery = 94% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl SpecificMix = 0406-15-01 Laboratory ID = 20171660002 Lab Value = 0.044 Expected Conc. = 0.04 Report level label = 0.008 Pct Recovery = 109% Analysis Date = 08/23/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = 060916 Laboratory ID = 20171380001 Lab Value = 0.032 Expected Conc. = 0.04 Report level label = 0.008 Pct Recovery = 80% Analysis Date = 06/07/17 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 041816 Laboratory ID = 20170740063 Lab Value = 0.034 Expected Conc. = 0.04 Report level label = 0.008 Pct Recovery = 86% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl SpecificMix = 041816 Laboratory ID = 20170190026 Lab Value = 0.043 Expected Conc. = 0.04 Report level label = 0.008 Pct Recovery = 107% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = 060916 Laboratory ID = 20161740258 Lab Value = 0.029 Expected Conc. = 0.04 Report level label = 0.008 Pct Recovery = 73% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 041816 Laboratory ID = 20142720002 Lab Value = 0.025 Expected Conc. = 0.0319 Report level label = 0.008 Pct Recovery = 78% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl SpecificMix = LC06435 Laboratory ID = 20142530087 Lab Value = 0.024 Expected Conc. = 0.0319 Report level label = 0.008 Pct Recovery = 74% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl SpecificMix = LC06435 Laboratory ID = 20141570088 Lab Value = 0.032 Expected Conc. = 0.0319 Report level label = 0.008 Pct Recovery = 99% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl SpecificMix = LC06435 Laboratory ID = 20141220025 Lab Value = 0.033 Expected Conc. = 0.0319 Report level label = 0.008 Pct Recovery = 104% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl SpecificMix = LC06435 Laboratory ID = 20150720069 Lab Value = 0.026 Expected Conc. = 0.0312 Report level label = 0.008 Pct Recovery = 83% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 03DD006 Laboratory ID = 20143110108 Lab Value = 0.022 Expected Conc. = 0.0312 Report level label = 0.008 Pct Recovery = 70% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 03DD006 Laboratory ID = 20142960086 Lab Value = 0.026 Expected Conc. = 0.0312 Report level label = 0.008 Pct Recovery = 83% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 03DD006 Laboratory ID = 20142270001 Lab Value = 0.025 Expected Conc. = 0.0312 Report level label = 0.008 Pct Recovery = 81% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl SpecificMix = 03DD006 Laboratory ID = 20173480003 Lab Value = 0.027 Expected Conc. = 0.0265 Report level label = 0.008 Pct Recovery = 103% Analysis Date = 04/05/18 SpikeMix = Abs 071717Pest: 50 µl & ChemService 6567600: 50 µl SpecificMix = 071717Pest Laboratory ID = 20172370001 Lab Value = 0.024 Expected Conc. = 0.0265 Report level label = 0.008 Pct Recovery = 91% Analysis Date = 11/18/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6537100: 50 µl SpecificMix = 6537100 Laboratory ID = 20172230001 Lab Value = 0.032 Expected Conc. = 0.0265 Report level label = 0.008 Pct Recovery = 120% Analysis Date = 10/19/17 SpikeMix = ChemService 6472100: 50 µl & Abs 071717Pest: 50 µl SpecificMix = 071717Pest Laboratory ID = 20160770090 Lab Value = 0.019 Expected Conc. = 0.0242 Report level label = 0.008 Pct Recovery = 79% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20160630046 Lab Value = 0.017 Expected Conc. = 0.0242 Report level label = 0.008 Pct Recovery = 70% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20153510109 Lab Value = 0.018 Expected Conc. = 0.0242 Report level label = 0.008 Pct Recovery = 74% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20153440001 Lab Value = 0.018 Expected Conc. = 0.0242 Report level label = 0.008 Pct Recovery = 74% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20161260151 Lab Value = 0.020 Expected Conc. = 0.024 Report level label = 0.008 Pct Recovery = 85% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = 3851600 Laboratory ID = 20151550293 Lab Value = 0.024 Expected Conc. = 0.024 Report level label = 0.008 Pct Recovery = 99% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl SpecificMix = 3851600 Laboratory ID = 20151270112 Lab Value = 0.020 Expected Conc. = 0.024 Report level label = 0.008 Pct Recovery = 85% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl SpecificMix = 3851600 Laboratory ID = 20172020035 Lab Value = 0.025 Expected Conc. = 0.0212 Report level label = 0.008 Pct Recovery = 116% Analysis Date = 11/07/17 SpikeMix = Abs 071717Pest: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 071717Pest Laboratory ID = 20171940002 Lab Value = 0.019 Expected Conc. = 0.02 Report level label = 0.008 Pct Recovery = 92% Analysis Date = 11/10/17 SpikeMix = ChemService 5054800: 40 µl & NSI 041816: 40 µl SpecificMix = 041816 Laboratory ID = 20171160110 Lab Value = 0.018 Expected Conc. = 0.02 Report level label = 0.008 Pct Recovery = 92% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = 060916 Laboratory ID = 20162520001 Lab Value = 0.023 Expected Conc. = 0.02 Report level label = 0.008 Pct Recovery = 114% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl SpecificMix = 060916 Laboratory ID = 20163560019 Lab Value = 0.018 Expected Conc. = 0.02 Report level label = 0.008 Pct Recovery = 89% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl SpecificMix = 060916 Laboratory ID = 20162380004 Lab Value = 0.021 Expected Conc. = 0.02 Report level label = 0.008 Pct Recovery = 106% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = 060916 Laboratory ID = 20162020124 Lab Value = 0.018 Expected Conc. = 0.02 Report level label = 0.008 Pct Recovery = 88% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl SpecificMix = 041816 Laboratory ID = 20161600087 Lab Value = 0.017 Expected Conc. = 0.02 Report level label = 0.008 Pct Recovery = 87% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 041816 Laboratory ID = 20161340228 Lab Value = 0.015 Expected Conc. = 0.02 Report level label = 0.008 Pct Recovery = 76% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl SpecificMix = 041816 Laboratory ID = 20161190075 Lab Value = 0.015 Expected Conc. = 0.02 Report level label = 0.008 Pct Recovery = 73% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 041816 Laboratory ID = 20150150115 Lab Value = 0.012 Expected Conc. = 0.016 Report level label = 0.008 Pct Recovery = 78% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl SpecificMix = LC06435 Laboratory ID = 20143370094 Lab Value = 0.012 Expected Conc. = 0.016 Report level label = 0.008 Pct Recovery = 72% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl SpecificMix = LC06435 Laboratory ID = 20141910243 Lab Value = 0.012 Expected Conc. = 0.016 Report level label = 0.008 Pct Recovery = 75% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = LC06435 Laboratory ID = 20141840097 Lab Value = 0.013 Expected Conc. = 0.016 Report level label = 0.008 Pct Recovery = 82% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl SpecificMix = LC06435 Laboratory ID = 20180940080 Lab Value = 0.017 Expected Conc. = 0.0159 Report level label = 0.008 Pct Recovery = 106% Analysis Date = 05/31/18 SpikeMix = ChemService 6472100: 30 µl & Abs 071717Pest: 30 µl SpecificMix = 071717Pest Laboratory ID = 20180730064 Lab Value = 0.021 Expected Conc. = 0.0159 Report level label = 0.008 Pct Recovery = 130% Analysis Date = 05/16/18 SpikeMix = Abs 071717Pest: 30 µl & Abs 071817Pest: 30 µl SpecificMix = 071717Pest Laboratory ID = 20173120093 Lab Value = 0.019 Expected Conc. = 0.0159 Report level label = 0.008 Pct Recovery = 118% Analysis Date = 03/10/18 SpikeMix = ChemService 6472100: 30 µl & ChemService 6537100: 30 µl SpecificMix = 6537100 Laboratory ID = 20172780018 Lab Value = 0.014 Expected Conc. = 0.0159 Report level label = 0.008 Pct Recovery = 86% Analysis Date = 02/08/18 SpikeMix = ChemService 6537100: 30 µl & Abs 071817Pest: 30 µl SpecificMix = 6537100 Laboratory ID = 20142200164 Lab Value = 0.015 Expected Conc. = 0.0156 Report level label = 0.008 Pct Recovery = 93% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 03DD006 Laboratory ID = 20141640076 Lab Value = 0.013 Expected Conc. = 0.0156 Report level label = 0.008 Pct Recovery = 85% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = 03DD006 Laboratory ID = 20141420140 Lab Value = 0.013 Expected Conc. = 0.0156 Report level label = 0.008 Pct Recovery = 82% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 03DD006 Laboratory ID = 20141080004 Lab Value = 0.014 Expected Conc. = 0.0156 Report level label = 0.008 Pct Recovery = 87% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl SpecificMix = 03DD006 Laboratory ID = 20152190003 Lab Value = 0.010 Expected Conc. = 0.0121 Report level label = 0.008 Pct Recovery = 84% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = 0406-15-01 Laboratory ID = 20152040177 Lab Value = 0.011 Expected Conc. = 0.0121 Report level label = 0.008 Pct Recovery = 88% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl SpecificMix = 0406-15-01 Laboratory ID = 20160430111 Lab Value = 0.013 Expected Conc. = 0.012 Report level label = 0.008 Pct Recovery = 108% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 3851600 Laboratory ID = 20160210080 Lab Value = 0.010 Expected Conc. = 0.012 Report level label = 0.008 Pct Recovery = 82% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 3851600 Laboratory ID = 20152950078 Lab Value = 0.008 Expected Conc. = 0.012 Report level label = 0.008 Pct Recovery = 67% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 3851600 Laboratory ID = 20153030068 Lab Value = 0.012 Expected Conc. = 0.012 Report level label = 0.008 Pct Recovery = 96% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = 3851600 Laboratory ID = 20151760208 Lab Value = 0.012 Expected Conc. = 0.012 Report level label = 0.008 Pct Recovery = 98% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl SpecificMix = 3851600 Laboratory ID = 20151380009 Lab Value = 0.010 Expected Conc. = 0.012 Report level label = 0.008 Pct Recovery = 87% Analysis Date = 05/30/15 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 3851600 Analysis Date = 05/31/18 Pct Recovery = 111% Analysis Date = 05/21/18 Pct Recovery = 110% Analysis Date = 05/21/18 Pct Recovery = 110% Analysis Date = 05/11/18 Pct Recovery = 110% Analysis Date = 05/11/18 Pct Recovery = 110% Analysis Date = 05/01/18 Pct Recovery = 110% Analysis Date = 05/01/18 Pct Recovery = 110% Analysis Date = 04/21/18 Pct Recovery = 109% Analysis Date = 04/21/18 Pct Recovery = 109% Analysis Date = 04/11/18 Pct Recovery = 109% Analysis Date = 04/11/18 Pct Recovery = 109% Analysis Date = 04/02/18 Pct Recovery = 109% Analysis Date = 04/02/18 Pct Recovery = 109% Analysis Date = 03/23/18 Pct Recovery = 108% Analysis Date = 03/23/18 Pct Recovery = 108% Analysis Date = 03/13/18 Pct Recovery = 108% Analysis Date = 03/13/18 Pct Recovery = 108% Analysis Date = 03/03/18 Pct Recovery = 108% Analysis Date = 03/03/18 Pct Recovery = 108% Analysis Date = 02/21/18 Pct Recovery = 107% Analysis Date = 02/21/18 Pct Recovery = 107% Analysis Date = 02/12/18 Pct Recovery = 107% Analysis Date = 02/12/18 Pct Recovery = 107% Analysis Date = 02/02/18 Pct Recovery = 107% Analysis Date = 02/02/18 Pct Recovery = 107% Analysis Date = 01/23/18 Pct Recovery = 106% Analysis Date = 01/23/18 Pct Recovery = 106% Analysis Date = 01/13/18 Pct Recovery = 106% Analysis Date = 01/13/18 Pct Recovery = 106% Analysis Date = 01/03/18 Pct Recovery = 106% Analysis Date = 01/03/18 Pct Recovery = 106% Analysis Date = 12/25/17 Pct Recovery = 105% Analysis Date = 12/25/17 Pct Recovery = 105% Analysis Date = 12/15/17 Pct Recovery = 105% Analysis Date = 12/15/17 Pct Recovery = 105% Analysis Date = 12/05/17 Pct Recovery = 105% Analysis Date = 12/05/17 Pct Recovery = 105% Analysis Date = 11/25/17 Pct Recovery = 104% Analysis Date = 11/25/17 Pct Recovery = 104% Analysis Date = 11/15/17 Pct Recovery = 104% Analysis Date = 11/15/17 Pct Recovery = 104% Analysis Date = 11/05/17 Pct Recovery = 104% Analysis Date = 11/05/17 Pct Recovery = 104% Analysis Date = 10/27/17 Pct Recovery = 104% Analysis Date = 10/27/17 Pct Recovery = 104% Analysis Date = 10/17/17 Pct Recovery = 103% Analysis Date = 10/17/17 Pct Recovery = 103% Analysis Date = 10/07/17 Pct Recovery = 103% Analysis Date = 10/07/17 Pct Recovery = 103% Analysis Date = 09/27/17 Pct Recovery = 103% Analysis Date = 09/27/17 Pct Recovery = 103% Analysis Date = 09/17/17 Pct Recovery = 102% Analysis Date = 09/17/17 Pct Recovery = 102% Analysis Date = 09/08/17 Pct Recovery = 102% Analysis Date = 09/08/17 Pct Recovery = 102% Analysis Date = 08/29/17 Pct Recovery = 102% Analysis Date = 08/29/17 Pct Recovery = 102% Analysis Date = 08/19/17 Pct Recovery = 101% Analysis Date = 08/19/17 Pct Recovery = 101% Analysis Date = 08/09/17 Pct Recovery = 101% Analysis Date = 08/09/17 Pct Recovery = 101% Analysis Date = 07/30/17 Pct Recovery = 101% Analysis Date = 07/30/17 Pct Recovery = 101% Analysis Date = 07/21/17 Pct Recovery = 100% Analysis Date = 07/21/17 Pct Recovery = 100% Analysis Date = 07/11/17 Pct Recovery = 100% Analysis Date = 07/11/17 Pct Recovery = 100% Analysis Date = 07/01/17 Pct Recovery = 100% Analysis Date = 07/01/17 Pct Recovery = 100% Analysis Date = 06/21/17 Pct Recovery = 99% Analysis Date = 06/21/17 Pct Recovery = 99% Analysis Date = 06/11/17 Pct Recovery = 99% Analysis Date = 06/11/17 Pct Recovery = 99% Analysis Date = 06/02/17 Pct Recovery = 99% Analysis Date = 06/02/17 Pct Recovery = 99% Analysis Date = 05/23/17 Pct Recovery = 98% Analysis Date = 05/23/17 Pct Recovery = 98% Analysis Date = 05/13/17 Pct Recovery = 98% Analysis Date = 05/13/17 Pct Recovery = 98% Analysis Date = 05/03/17 Pct Recovery = 98% Analysis Date = 05/03/17 Pct Recovery = 98% Analysis Date = 04/23/17 Pct Recovery = 97% Analysis Date = 04/23/17 Pct Recovery = 97% Analysis Date = 04/13/17 Pct Recovery = 97% Analysis Date = 04/13/17 Pct Recovery = 97% Analysis Date = 04/04/17 Pct Recovery = 97% Analysis Date = 04/04/17 Pct Recovery = 97% Analysis Date = 03/25/17 Pct Recovery = 97% Analysis Date = 03/25/17 Pct Recovery = 97% Analysis Date = 03/15/17 Pct Recovery = 96% Analysis Date = 03/15/17 Pct Recovery = 96% Analysis Date = 03/05/17 Pct Recovery = 96% Analysis Date = 03/05/17 Pct Recovery = 96% Analysis Date = 02/23/17 Pct Recovery = 96% Analysis Date = 02/23/17 Pct Recovery = 96% Analysis Date = 02/14/17 Pct Recovery = 95% Analysis Date = 02/14/17 Pct Recovery = 95% Analysis Date = 02/04/17 Pct Recovery = 95% Analysis Date = 02/04/17 Pct Recovery = 95% Analysis Date = 01/25/17 Pct Recovery = 95% Analysis Date = 01/25/17 Pct Recovery = 95% Analysis Date = 01/15/17 Pct Recovery = 94% Analysis Date = 01/15/17 Pct Recovery = 94% Analysis Date = 01/05/17 Pct Recovery = 94% Analysis Date = 01/05/17 Pct Recovery = 94% Analysis Date = 12/27/16 Pct Recovery = 94% Analysis Date = 12/27/16 Pct Recovery = 94% Analysis Date = 12/17/16 Pct Recovery = 94% Analysis Date = 12/17/16 Pct Recovery = 94% Analysis Date = 12/07/16 Pct Recovery = 93% Analysis Date = 12/07/16 Pct Recovery = 93% Analysis Date = 11/27/16 Pct Recovery = 93% Analysis Date = 11/27/16 Pct Recovery = 93% Analysis Date = 11/17/16 Pct Recovery = 93% Analysis Date = 11/17/16 Pct Recovery = 93% Analysis Date = 11/08/16 Pct Recovery = 92% Analysis Date = 11/08/16 Pct Recovery = 92% Analysis Date = 10/29/16 Pct Recovery = 92% Analysis Date = 10/29/16 Pct Recovery = 92% Analysis Date = 10/19/16 Pct Recovery = 92% Analysis Date = 10/19/16 Pct Recovery = 92% Analysis Date = 10/09/16 Pct Recovery = 92% Analysis Date = 10/09/16 Pct Recovery = 92% Analysis Date = 09/29/16 Pct Recovery = 91% Analysis Date = 09/29/16 Pct Recovery = 91% Analysis Date = 09/19/16 Pct Recovery = 91% Analysis Date = 09/19/16 Pct Recovery = 91% Analysis Date = 09/10/16 Pct Recovery = 91% Analysis Date = 09/10/16 Pct Recovery = 91% Analysis Date = 08/31/16 Pct Recovery = 91% Analysis Date = 08/31/16 Pct Recovery = 91% Analysis Date = 08/21/16 Pct Recovery = 90% Analysis Date = 08/21/16 Pct Recovery = 90% Analysis Date = 08/11/16 Pct Recovery = 90% Analysis Date = 08/11/16 Pct Recovery = 90% Analysis Date = 08/01/16 Pct Recovery = 90% Analysis Date = 08/01/16 Pct Recovery = 90% Analysis Date = 07/23/16 Pct Recovery = 90% Analysis Date = 07/23/16 Pct Recovery = 90% Analysis Date = 07/13/16 Pct Recovery = 89% Analysis Date = 07/13/16 Pct Recovery = 89% Analysis Date = 07/03/16 Pct Recovery = 89% Analysis Date = 07/03/16 Pct Recovery = 89% Analysis Date = 06/23/16 Pct Recovery = 89% Analysis Date = 06/23/16 Pct Recovery = 89% Analysis Date = 06/13/16 Pct Recovery = 89% Analysis Date = 06/13/16 Pct Recovery = 89% Analysis Date = 06/04/16 Pct Recovery = 88% Analysis Date = 06/04/16 Pct Recovery = 88% Analysis Date = 05/25/16 Pct Recovery = 88% Analysis Date = 05/25/16 Pct Recovery = 88% Analysis Date = 05/15/16 Pct Recovery = 88% Analysis Date = 05/15/16 Pct Recovery = 88% Analysis Date = 05/05/16 Pct Recovery = 88% Analysis Date = 05/05/16 Pct Recovery = 88% Analysis Date = 04/25/16 Pct Recovery = 87% Analysis Date = 04/25/16 Pct Recovery = 87% Analysis Date = 04/16/16 Pct Recovery = 87% Analysis Date = 04/16/16 Pct Recovery = 87% Analysis Date = 04/06/16 Pct Recovery = 87% Analysis Date = 04/06/16 Pct Recovery = 87% Analysis Date = 03/27/16 Pct Recovery = 87% Analysis Date = 03/27/16 Pct Recovery = 87% Analysis Date = 03/17/16 Pct Recovery = 86% Analysis Date = 03/17/16 Pct Recovery = 86% Analysis Date = 03/07/16 Pct Recovery = 86% Analysis Date = 03/07/16 Pct Recovery = 86% Analysis Date = 02/26/16 Pct Recovery = 86% Analysis Date = 02/26/16 Pct Recovery = 86% Analysis Date = 02/17/16 Pct Recovery = 86% Analysis Date = 02/17/16 Pct Recovery = 86% Analysis Date = 02/07/16 Pct Recovery = 86% Analysis Date = 02/07/16 Pct Recovery = 86% Analysis Date = 01/28/16 Pct Recovery = 86% Analysis Date = 01/28/16 Pct Recovery = 86% Analysis Date = 01/18/16 Pct Recovery = 85% Analysis Date = 01/18/16 Pct Recovery = 85% Analysis Date = 01/08/16 Pct Recovery = 85% Analysis Date = 01/08/16 Pct Recovery = 85% Analysis Date = 12/30/15 Pct Recovery = 85% Analysis Date = 12/30/15 Pct Recovery = 85% Analysis Date = 12/20/15 Pct Recovery = 85% Analysis Date = 12/20/15 Pct Recovery = 85% Analysis Date = 12/10/15 Pct Recovery = 85% Analysis Date = 12/10/15 Pct Recovery = 85% Analysis Date = 11/30/15 Pct Recovery = 84% Analysis Date = 11/30/15 Pct Recovery = 84% Analysis Date = 11/20/15 Pct Recovery = 84% Analysis Date = 11/20/15 Pct Recovery = 84% Analysis Date = 11/11/15 Pct Recovery = 84% Analysis Date = 11/11/15 Pct Recovery = 84% Analysis Date = 11/01/15 Pct Recovery = 84% Analysis Date = 11/01/15 Pct Recovery = 84% Analysis Date = 10/22/15 Pct Recovery = 84% Analysis Date = 10/22/15 Pct Recovery = 84% Analysis Date = 10/12/15 Pct Recovery = 84% Analysis Date = 10/12/15 Pct Recovery = 84% Analysis Date = 10/02/15 Pct Recovery = 83% Analysis Date = 10/02/15 Pct Recovery = 83% Analysis Date = 09/23/15 Pct Recovery = 83% Analysis Date = 09/23/15 Pct Recovery = 83% Analysis Date = 09/13/15 Pct Recovery = 83% Analysis Date = 09/13/15 Pct Recovery = 83% Analysis Date = 09/03/15 Pct Recovery = 83% Analysis Date = 09/03/15 Pct Recovery = 83% Analysis Date = 08/24/15 Pct Recovery = 83% Analysis Date = 08/24/15 Pct Recovery = 83% Analysis Date = 08/14/15 Pct Recovery = 83% Analysis Date = 08/14/15 Pct Recovery = 83% Analysis Date = 08/04/15 Pct Recovery = 83% Analysis Date = 08/04/15 Pct Recovery = 83% Analysis Date = 07/26/15 Pct Recovery = 83% Analysis Date = 07/26/15 Pct Recovery = 83% Analysis Date = 07/16/15 Pct Recovery = 83% Analysis Date = 07/16/15 Pct Recovery = 83% Analysis Date = 07/06/15 Pct Recovery = 83% Analysis Date = 07/06/15 Pct Recovery = 83% Analysis Date = 06/26/15 Pct Recovery = 83% Analysis Date = 06/26/15 Pct Recovery = 83% Analysis Date = 06/16/15 Pct Recovery = 83% Analysis Date = 06/16/15 Pct Recovery = 83% Analysis Date = 06/07/15 Pct Recovery = 83% Analysis Date = 06/07/15 Pct Recovery = 83% Analysis Date = 05/28/15 Pct Recovery = 83% Analysis Date = 05/28/15 Pct Recovery = 83% Analysis Date = 05/18/15 Pct Recovery = 83% Analysis Date = 05/18/15 Pct Recovery = 83% Analysis Date = 05/08/15 Pct Recovery = 84% Analysis Date = 05/08/15 Pct Recovery = 84% Analysis Date = 04/28/15 Pct Recovery = 84% Analysis Date = 04/28/15 Pct Recovery = 84% Analysis Date = 04/19/15 Pct Recovery = 84% Analysis Date = 04/19/15 Pct Recovery = 84% Analysis Date = 04/09/15 Pct Recovery = 84% Analysis Date = 04/09/15 Pct Recovery = 84% Analysis Date = 03/30/15 Pct Recovery = 84% Analysis Date = 03/30/15 Pct Recovery = 84% Analysis Date = 03/20/15 Pct Recovery = 84% Analysis Date = 03/20/15 Pct Recovery = 84% Analysis Date = 03/10/15 Pct Recovery = 84% Analysis Date = 03/10/15 Pct Recovery = 84% Analysis Date = 02/28/15 Pct Recovery = 84% Analysis Date = 02/28/15 Pct Recovery = 84% Analysis Date = 02/19/15 Pct Recovery = 84% Analysis Date = 02/19/15 Pct Recovery = 84% Analysis Date = 02/09/15 Pct Recovery = 84% Analysis Date = 02/09/15 Pct Recovery = 84% Analysis Date = 01/30/15 Pct Recovery = 84% Analysis Date = 01/30/15 Pct Recovery = 84% Analysis Date = 01/20/15 Pct Recovery = 85% Analysis Date = 01/20/15 Pct Recovery = 85% Analysis Date = 01/10/15 Pct Recovery = 85% Analysis Date = 01/10/15 Pct Recovery = 85% Analysis Date = 01/01/15 Pct Recovery = 85% Analysis Date = 01/01/15 Pct Recovery = 85% Analysis Date = 12/22/14 Pct Recovery = 85% Analysis Date = 12/22/14 Pct Recovery = 85% Analysis Date = 12/12/14 Pct Recovery = 85% Analysis Date = 12/12/14 Pct Recovery = 85% Analysis Date = 12/02/14 Pct Recovery = 85% Analysis Date = 12/02/14 Pct Recovery = 85% Analysis Date = 11/22/14 Pct Recovery = 85% Analysis Date = 11/22/14 Pct Recovery = 85% Analysis Date = 11/13/14 Pct Recovery = 85% Analysis Date = 11/13/14 Pct Recovery = 85% Analysis Date = 11/03/14 Pct Recovery = 85% Analysis Date = 11/03/14 Pct Recovery = 85% Analysis Date = 10/24/14 Pct Recovery = 86% Analysis Date = 10/24/14 Pct Recovery = 86% Analysis Date = 10/14/14 Pct Recovery = 86% Analysis Date = 10/14/14 Pct Recovery = 86% Analysis Date = 10/04/14 Pct Recovery = 86% Analysis Date = 10/04/14 Pct Recovery = 86% Analysis Date = 09/25/14 Pct Recovery = 86% Analysis Date = 09/25/14 Pct Recovery = 86% Analysis Date = 09/15/14 Pct Recovery = 86% Analysis Date = 09/15/14 Pct Recovery = 86% Analysis Date = 09/05/14 Pct Recovery = 86% Analysis Date = 09/05/14 Pct Recovery = 86% Analysis Date = 08/26/14 Pct Recovery = 87% Analysis Date = 08/26/14 Pct Recovery = 87% Analysis Date = 08/16/14 Pct Recovery = 87% Analysis Date = 08/16/14 Pct Recovery = 87% Analysis Date = 08/06/14 Pct Recovery = 87% Analysis Date = 08/06/14 Pct Recovery = 87% Analysis Date = 07/28/14 Pct Recovery = 87% Analysis Date = 07/28/14 Pct Recovery = 87% Analysis Date = 07/18/14 Pct Recovery = 88% Analysis Date = 07/18/14 Pct Recovery = 88% Analysis Date = 07/08/14 Pct Recovery = 88% Analysis Date = 07/08/14 Pct Recovery = 88% Analysis Date = 06/28/14 Pct Recovery = 88% Analysis Date = 06/28/14 Pct Recovery = 88% Analysis Date = 06/18/14 Pct Recovery = 88% Analysis Date = 06/18/14 Pct Recovery = 88% Analysis Date = 06/09/14 Pct Recovery = 89% Analysis Date = 06/09/14 Pct Recovery = 89% Analysis Date = 05/30/14 Pct Recovery = 89% Analysis Date = 05/30/14 Pct Recovery = 89% Analysis Date = 05/20/14 Pct Recovery = 89% Analysis Date = 05/20/14 Pct Recovery = 89% Analysis Date = 05/10/14 Pct Recovery = 89% Analysis Date = 05/10/14 Pct Recovery = 89% Analysis Date = 04/30/14 Pct Recovery = 90% Analysis Date = 04/30/14 Pct Recovery = 90% Analysis Date = 04/21/14 Pct Recovery = 90% Analysis Date = 04/21/14 Pct Recovery = 90% Analysis Date = 04/11/14 Pct Recovery = 90% Analysis Date = 04/11/14 Pct Recovery = 90% Analysis Date = 04/01/14 Pct Recovery = 90% Analysis Date = 04/01/14 Pct Recovery = 90% Analysis Date = 03/22/14 Pct Recovery = 91% Analysis Date = 03/22/14 Pct Recovery = 91% Analysis Date = 03/12/14 Pct Recovery = 91% Analysis Date = 03/12/14 Pct Recovery = 91% Analysis Date = 03/03/14 Pct Recovery = 91% Analysis Date = 03/03/14 Pct Recovery = 91% Analysis Date = 02/21/14 Pct Recovery = 91% Analysis Date = 02/21/14 Pct Recovery = 91% Analysis Date = 02/11/14 Pct Recovery = 92% Analysis Date = 02/11/14 Pct Recovery = 92% Analysis Date = 02/01/14 Pct Recovery = 92% Analysis Date = 02/01/14 Pct Recovery = 92% Analysis Date = 01/22/14 Pct Recovery = 92% Analysis Date = 01/22/14 Pct Recovery = 92% Analysis Date = 01/12/14 Pct Recovery = 92% Analysis Date = 01/12/14 Pct Recovery = 92% Analysis Date = 01/03/14 Pct Recovery = 93% Analysis Date = 01/03/14 Pct Recovery = 93% Analysis Date = 12/24/13 Pct Recovery = 93% Analysis Date = 12/24/13 Pct Recovery = 93% Analysis Date = 12/14/13 Pct Recovery = 93% Analysis Date = 12/14/13 Pct Recovery = 93% Analysis Date = 12/04/13 Pct Recovery = 93% Analysis Date = 12/04/13 Pct Recovery = 93% Analysis Date = 11/24/13 Pct Recovery = 93% Analysis Date = 11/24/13 Pct Recovery = 93% Analysis Date = 11/15/13 Pct Recovery = 94% Analysis Date = 11/15/13 Pct Recovery = 94% Analysis Date = 11/05/13 Pct Recovery = 94% Analysis Date = 11/05/13 Pct Recovery = 94% Analysis Date = 10/26/13 Pct Recovery = 94% Analysis Date = 10/26/13 Pct Recovery = 94% Analysis Date = 10/16/13 Pct Recovery = 94% Analysis Date = 10/16/13 Pct Recovery = 94% Analysis Date = 10/06/13 Pct Recovery = 95% Analysis Date = 10/06/13 Pct Recovery = 95% Analysis Date = 09/27/13 Pct Recovery = 95% Analysis Date = 09/27/13 Pct Recovery = 95% Analysis Date = 09/17/13 Pct Recovery = 95% Analysis Date = 09/17/13 Pct Recovery = 95% Analysis Date = 09/07/13 Pct Recovery = 95% Analysis Date = 09/07/13 Pct Recovery = 95% Analysis Date = 08/28/13 Pct Recovery = 96% Analysis Date = 08/28/13 Pct Recovery = 96% Analysis Date = 08/18/13 Pct Recovery = 96% Analysis Date = 08/18/13 Pct Recovery = 96% Analysis Date = 08/09/13 Pct Recovery = 96% Analysis Date = 08/09/13 Pct Recovery = 96% Analysis Date = 07/30/13 Pct Recovery = 96% Analysis Date = 07/30/13 Pct Recovery = 96% Analysis Date = 07/20/13 Pct Recovery = 97% Analysis Date = 07/20/13 Pct Recovery = 97% Analysis Date = 07/10/13 Pct Recovery = 97% Analysis Date = 07/10/13 Pct Recovery = 97% Analysis Date = 06/30/13 Pct Recovery = 97% Analysis Date = 06/30/13 Pct Recovery = 97% Analysis Date = 06/20/13 Pct Recovery = 97% Analysis Date = 06/20/13 Pct Recovery = 97% Analysis Date = 06/11/13 Pct Recovery = 97% Analysis Date = 06/11/13 Pct Recovery = 97% Analysis Date = 06/01/13 Pct Recovery = 98% Analysis Date = 06/01/13 Pct Recovery = 98% Analysis Date = 05/22/13 Pct Recovery = 98% Analysis Date = 05/22/13 Pct Recovery = 98% Analysis Date = 05/12/13 Pct Recovery = 98% Analysis Date = 05/12/13 Pct Recovery = 98% Analysis Date = 05/02/13 Pct Recovery = 98% Analysis Date = 05/02/13 Pct Recovery = 98% Analysis Date = 04/23/13 Pct Recovery = 99% Analysis Date = 04/23/13 Pct Recovery = 99% Analysis Date = 04/13/13 Pct Recovery = 99% Analysis Date = 04/13/13 Pct Recovery = 99% Analysis Date = 04/03/13 Pct Recovery = 99% Analysis Date = 04/03/13 Pct Recovery = 99% Analysis Date = 03/24/13 Pct Recovery = 99% Analysis Date = 03/24/13 Pct Recovery = 99% Analysis Date = 03/14/13 Pct Recovery = 100% Analysis Date = 03/14/13 Pct Recovery = 100% Analysis Date = 03/05/13 Pct Recovery = 100% Analysis Date = 03/05/13 Pct Recovery = 100% Analysis Date = 02/23/13 Pct Recovery = 100% Analysis Date = 02/23/13 Pct Recovery = 100% Analysis Date = 02/13/13 Pct Recovery = 100% Analysis Date = 02/13/13 Pct Recovery = 100% Analysis Date = 02/03/13 Pct Recovery = 101% Analysis Date = 02/03/13 Pct Recovery = 101% Analysis Date = 01/24/13 Pct Recovery = 101% Analysis Date = 01/24/13 Pct Recovery = 101% Analysis Date = 01/15/13 Pct Recovery = 101% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
ATRAZINE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 83 92% 15% 90% 17%
Total 83 92% 15% 90% 17%

Sample Statistics
ATRAZINE

Characteristic N % % Basis
Plotted 83 100% Spiked
Estimated Values 3 4% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 83 .  
False Negatives 0 0% 0 out of 83
Not Spiked 51 .  
False Positives 0 0% 0 out of 51

OBSP Determination:
AZINPHOS-METHYL
METHOD: 2033 , TESTIDCODE: 82686GCM35

Laboratory ID = 20140100085 Lab Value = 0.966 Expected Conc. = 1.006 Report level label = 0.12 Pct Recovery = 96% Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl SpecificMix = 042413 Laboratory ID = 20172510330 Lab Value = 0.712 Expected Conc. = 0.81 Report level label = 0.12 Pct Recovery = 88% Analysis Date = 12/29/17 SpikeMix = ChemService 6537100: 100 µl & Abs 071817Pest: 100 µl SpecificMix = 6537100 Laboratory ID = 20180390003 Lab Value = 0.618 Expected Conc. = 0.804 Report level label = 0.12 Pct Recovery = 77% Analysis Date = 04/06/18 SpikeMix = Spex Organics EN170808006: 100 µl & Abs 071717Pest: 100 µl SpecificMix = 071717Pest Laboratory ID = 20162860079 Lab Value = 0.482 Expected Conc. = 0.75 Report level label = 0.12 Pct Recovery = 64% Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl SpecificMix = 5054800 Laboratory ID = 20163370001 Lab Value = 0.498 Expected Conc. = 0.75 Report level label = 0.12 Pct Recovery = 66% Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl SpecificMix = LC20138V Laboratory ID = 20161880109 Lab Value = 0.693 Expected Conc. = 0.75 Report level label = 0.12 Pct Recovery = 92% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl SpecificMix = 5054800 Laboratory ID = 20152750006 Lab Value = 0.408 Expected Conc. = 0.72 Report level label = 0.12 Pct Recovery = 57% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl SpecificMix = EN150514012 Laboratory ID = 20152460215 Lab Value = 0.430 Expected Conc. = 0.72 Report level label = 0.12 Pct Recovery = 60% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl SpecificMix = EN150514012 Laboratory ID = 20171720140 Lab Value = 0.489 Expected Conc. = 0.6 Report level label = 0.12 Pct Recovery = 82% Analysis Date = 08/31/17 SpikeMix = Supelco LC20138V: 80 µl & Phenova B20160331: 80 µl SpecificMix = LC20138V Laboratory ID = 20171380001 Lab Value = 0.283 Expected Conc. = 0.6 Report level label = 0.12 Pct Recovery = 47% Analysis Date = 06/07/17 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 5054800 Laboratory ID = 20170960001 Lab Value = 0.406 Expected Conc. = 0.6 Report level label = 0.12 Pct Recovery = 68% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl SpecificMix = 5054800 Laboratory ID = 20170740063 Lab Value = 0.441 Expected Conc. = 0.6 Report level label = 0.12 Pct Recovery = 74% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl SpecificMix = LC20138V Laboratory ID = 20161740258 Lab Value = 0.367 Expected Conc. = 0.6 Report level label = 0.12 Pct Recovery = 61% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 5054800 Laboratory ID = 20161470001 Lab Value = 0.518 Expected Conc. = 0.6 Report level label = 0.12 Pct Recovery = 86% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl SpecificMix = LC20138V Laboratory ID = 20130250061 Lab Value = 0.493 Expected Conc. = 0.597 Report level label = 0.12 Pct Recovery = 83% Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl SpecificMix = 05BB029 Laboratory ID = 20132690010 Lab Value = 0.391 Expected Conc. = 0.503 Report level label = 0.12 Pct Recovery = 78% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl SpecificMix = 042413 Laboratory ID = 20132560001 Lab Value = 0.277 Expected Conc. = 0.503 Report level label = 0.12 Pct Recovery = 55% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl SpecificMix = 042413 Laboratory ID = 20132140002 Lab Value = 0.281 Expected Conc. = 0.4945 Report level label = 0.12 Pct Recovery = 57% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl SpecificMix = 04CC101 Laboratory ID = 20150720069 Lab Value = 0.370 Expected Conc. = 0.4878 Report level label = 0.12 Pct Recovery = 76% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 0227-14-08 Laboratory ID = 20141770149 Lab Value = 0.276 Expected Conc. = 0.4878 Report level label = 0.12 Pct Recovery = 57% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl SpecificMix = 0227-14-08 Laboratory ID = 20141570088 Lab Value = 0.362 Expected Conc. = 0.4878 Report level label = 0.12 Pct Recovery = 74% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl SpecificMix = 0227-14-08 Laboratory ID = 20150430092 Lab Value = 0.306 Expected Conc. = 0.4794 Report level label = 0.12 Pct Recovery = 64% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl SpecificMix = 042814 Laboratory ID = 20143240095 Lab Value = 0.381 Expected Conc. = 0.4794 Report level label = 0.12 Pct Recovery = 79% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl SpecificMix = 042814 Laboratory ID = 20142960086 Lab Value = 0.255 Expected Conc. = 0.4794 Report level label = 0.12 Pct Recovery = 53% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 042814 Laboratory ID = 20142530087 Lab Value = 0.204 Expected Conc. = 0.4794 Report level label = 0.12 Pct Recovery = 43% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl SpecificMix = 042814 Laboratory ID = 20172370001 Lab Value = 0.366 Expected Conc. = 0.405 Report level label = 0.12 Pct Recovery = 90% Analysis Date = 11/18/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6537100: 50 µl SpecificMix = 6537100 Laboratory ID = 20173480003 Lab Value = 0.254 Expected Conc. = 0.402 Report level label = 0.12 Pct Recovery = 63% Analysis Date = 04/05/18 SpikeMix = Abs 071717Pest: 50 µl & ChemService 6567600: 50 µl SpecificMix = 071717Pest Laboratory ID = 20172230001 Lab Value = 0.337 Expected Conc. = 0.402 Report level label = 0.12 Pct Recovery = 84% Analysis Date = 10/19/17 SpikeMix = ChemService 6472100: 50 µl & Abs 071717Pest: 50 µl SpecificMix = 071717Pest Laboratory ID = 20152330039 Lab Value = 0.228 Expected Conc. = 0.3612 Report level label = 0.12 Pct Recovery = 63% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl SpecificMix = 041415 Laboratory ID = 20151900132 Lab Value = 0.215 Expected Conc. = 0.3612 Report level label = 0.12 Pct Recovery = 60% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl SpecificMix = 041415 Laboratory ID = 20151270112 Lab Value = 0.219 Expected Conc. = 0.3612 Report level label = 0.12 Pct Recovery = 61% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl SpecificMix = 041415 Laboratory ID = 20160630046 Lab Value = 0.184 Expected Conc. = 0.36 Report level label = 0.12 Pct Recovery = 51% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = EN150514012 Laboratory ID = 20153440001 Lab Value = 0.222 Expected Conc. = 0.36 Report level label = 0.12 Pct Recovery = 62% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = EN150514012 Laboratory ID = 20172020035 Lab Value = 0.290 Expected Conc. = 0.3216 Report level label = 0.12 Pct Recovery = 90% Analysis Date = 11/07/17 SpikeMix = Abs 071717Pest: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 071717Pest Laboratory ID = 20130940097 Lab Value = 0.151 Expected Conc. = 0.3015 Report level label = 0.12 Pct Recovery = 50% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = 052412 Laboratory ID = 20130100066 Lab Value = 0.261 Expected Conc. = 0.3015 Report level label = 0.12 Pct Recovery = 87% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl SpecificMix = 052412 Laboratory ID = 20140230082 Lab Value = 0.189 Expected Conc. = 0.301 Report level label = 0.12 Pct Recovery = 63% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl SpecificMix = 012513 Laboratory ID = 20132420001 Lab Value = 0.213 Expected Conc. = 0.301 Report level label = 0.12 Pct Recovery = 71% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl SpecificMix = 012513 Laboratory ID = 20171940002 Lab Value = 0.202 Expected Conc. = 0.3 Report level label = 0.12 Pct Recovery = 67% Analysis Date = 11/10/17 SpikeMix = ChemService 5054800: 40 µl & NSI 041816: 40 µl SpecificMix = 5054800 Laboratory ID = 20171510080 Lab Value = 0.205 Expected Conc. = 0.3 Report level label = 0.12 Pct Recovery = 68% Analysis Date = 06/09/17 SpikeMix = Supelco LC20138V: 40 µl & Crescent 03FF076: 40 µl SpecificMix = LC20138V Laboratory ID = 20170460061 Lab Value = 0.198 Expected Conc. = 0.3 Report level label = 0.12 Pct Recovery = 66% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl SpecificMix = 5054800 Laboratory ID = 20162520001 Lab Value = 0.268 Expected Conc. = 0.3 Report level label = 0.12 Pct Recovery = 89% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl SpecificMix = LC20138V Laboratory ID = 20163560019 Lab Value = 0.198 Expected Conc. = 0.3 Report level label = 0.12 Pct Recovery = 66% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl SpecificMix = 5054800 Laboratory ID = 20162660005 Lab Value = 0.195 Expected Conc. = 0.3 Report level label = 0.12 Pct Recovery = 65% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl SpecificMix = LC20138V Laboratory ID = 20162150213 Lab Value = 0.243 Expected Conc. = 0.3 Report level label = 0.12 Pct Recovery = 81% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl SpecificMix = 5054800 Laboratory ID = 20162020124 Lab Value = 0.167 Expected Conc. = 0.3 Report level label = 0.12 Pct Recovery = 56% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl SpecificMix = LC20138V Laboratory ID = 20141840097 Lab Value = 0.101 Expected Conc. = 0.2439 Report level label = 0.12 Pct Recovery = 41% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20141490205 Lab Value = 0.174 Expected Conc. = 0.2439 Report level label = 0.12 Pct Recovery = 71% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20141420140 Lab Value = 0.194 Expected Conc. = 0.2439 Report level label = 0.12 Pct Recovery = 80% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20141360094 Lab Value = 0.112 Expected Conc. = 0.2439 Report level label = 0.12 Pct Recovery = 46% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20173120093 Lab Value = 0.212 Expected Conc. = 0.243 Report level label = 0.12 Pct Recovery = 87% Analysis Date = 03/10/18 SpikeMix = ChemService 6472100: 30 µl & ChemService 6537100: 30 µl SpecificMix = 6537100 Laboratory ID = 20172780018 Lab Value = 0.182 Expected Conc. = 0.243 Report level label = 0.12 Pct Recovery = 75% Analysis Date = 02/08/18 SpikeMix = ChemService 6537100: 30 µl & Abs 071817Pest: 30 µl SpecificMix = 6537100 Laboratory ID = 20180940080 Lab Value = 0.164 Expected Conc. = 0.2412 Report level label = 0.12 Pct Recovery = 68% Analysis Date = 05/31/18 SpikeMix = ChemService 6472100: 30 µl & Abs 071717Pest: 30 µl SpecificMix = 071717Pest Laboratory ID = 20180730064 Lab Value = 0.240 Expected Conc. = 0.2412 Report level label = 0.12 Pct Recovery = 100% Analysis Date = 05/16/18 SpikeMix = Abs 071717Pest: 30 µl & Abs 071817Pest: 30 µl SpecificMix = 071717Pest Laboratory ID = 20143370094 Lab Value = 0.133 Expected Conc. = 0.2397 Report level label = 0.12 Pct Recovery = 55% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl SpecificMix = 042814 Laboratory ID = 20142820151 Lab Value = 0.154 Expected Conc. = 0.2397 Report level label = 0.12 Pct Recovery = 64% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl SpecificMix = 042814 Laboratory ID = 20142470041 Lab Value = 0.146 Expected Conc. = 0.2397 Report level label = 0.12 Pct Recovery = 61% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl SpecificMix = 042814 Laboratory ID = 20142200164 Lab Value = 0.128 Expected Conc. = 0.2397 Report level label = 0.12 Pct Recovery = 53% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 042814 Laboratory ID = 20133580036 Lab Value = 0.126 Expected Conc. = 0.2012 Report level label = 0.12 Pct Recovery = 63% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 042413 Laboratory ID = 20133190012 Lab Value = 0.198 Expected Conc. = 0.2012 Report level label = 0.12 Pct Recovery = 98% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 042413 Laboratory ID = 20131650073 Lab Value = 0.218 Expected Conc. = 0.2012 Report level label = 0.12 Pct Recovery = 108% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl SpecificMix = 042413 Laboratory ID = 20140730138 Lab Value = 0.126 Expected Conc. = 0.1978 Report level label = 0.12 Pct Recovery = 64% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 04CC101 Laboratory ID = 20140510043 Lab Value = 0.102 Expected Conc. = 0.1978 Report level label = 0.12 Pct Recovery = 52% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 04CC101 Laboratory ID = 20133310030 Lab Value = 0.223 Expected Conc. = 0.1978 Report level label = 0.12 Pct Recovery = 113% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl SpecificMix = 04CC101 Laboratory ID = 20132280016 Lab Value = 0.185 Expected Conc. = 0.1978 Report level label = 0.12 Pct Recovery = 94% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl SpecificMix = 04CC101 Laboratory ID = 20131510026 Lab Value = 0.145 Expected Conc. = 0.1978 Report level label = 0.12 Pct Recovery = 73% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl SpecificMix = 04CC101 Laboratory ID = 20161050143 Lab Value = 0.139 Expected Conc. = 0.1806 Report level label = 0.12 Pct Recovery = 77% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 041415 Laboratory ID = 20160560044 Lab Value = 0.111 Expected Conc. = 0.1806 Report level label = 0.12 Pct Recovery = 61% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl SpecificMix = 041415 Laboratory ID = 20160210080 Lab Value = 0.082 Expected Conc. = 0.1806 Report level label = 0.12 Pct Recovery = 45% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 041415 Laboratory ID = 20152950078 Lab Value = 0.107 Expected Conc. = 0.1806 Report level label = 0.12 Pct Recovery = 59% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 041415 Laboratory ID = 20152040177 Lab Value = 0.109 Expected Conc. = 0.1806 Report level label = 0.12 Pct Recovery = 60% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl SpecificMix = 041415 Laboratory ID = 20151210037 Lab Value = 0.108 Expected Conc. = 0.1806 Report level label = 0.12 Pct Recovery = 60% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 041415 Laboratory ID = 20160070059 Lab Value = 0.114 Expected Conc. = 0.18 Report level label = 0.12 Pct Recovery = 63% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = EN150514012 Laboratory ID = 20153160001 Lab Value = 0.113 Expected Conc. = 0.18 Report level label = 0.12 Pct Recovery = 63% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = EN150514012 Laboratory ID = 20151760208 Lab Value = 0.096 Expected Conc. = 0.18 Report level label = 0.12 Pct Recovery = 53% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl SpecificMix = EN150514012 Laboratory ID = 20151480170 Lab Value = 0.147 Expected Conc. = 0.18 Report level label = 0.12 Pct Recovery = 82% Analysis Date = 06/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150514012 Laboratory ID = 20133400002 Lab Value = 0.091 Expected Conc. = 0.1206 Report level label = 0.12 Pct Recovery = 75% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = 052412 Laboratory ID = 20132910008 Lab Value = 0.060 Expected Conc. = 0.1206 Report level label = 0.12 Pct Recovery = 50% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = 052412 Laboratory ID = 20130650005 Lab Value = 0.077 Expected Conc. = 0.1206 Report level label = 0.12 Pct Recovery = 64% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl SpecificMix = 052412 Laboratory ID = 20140860102 Lab Value = 0.082 Expected Conc. = 0.1204 Report level label = 0.12 Pct Recovery = 68% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 012513 Laboratory ID = 20131920149 Lab Value = 0.089 Expected Conc. = 0.1204 Report level label = 0.12 Pct Recovery = 74% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl SpecificMix = 012513 Laboratory ID = 20131230084 Lab Value = 0.118 Expected Conc. = 0.1194 Report level label = 0.12 Pct Recovery = 99% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl SpecificMix = 05BB029 Laboratory ID = 20130510051 Lab Value = 0.112 Expected Conc. = 0.1194 Report level label = 0.12 Pct Recovery = 94% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl SpecificMix = 05BB029 Analysis Date = 05/30/18 Pct Recovery = 82% Analysis Date = 05/21/18 Pct Recovery = 81% Analysis Date = 05/21/18 Pct Recovery = 81% Analysis Date = 05/11/18 Pct Recovery = 81% Analysis Date = 05/11/18 Pct Recovery = 81% Analysis Date = 05/01/18 Pct Recovery = 81% Analysis Date = 05/01/18 Pct Recovery = 81% Analysis Date = 04/21/18 Pct Recovery = 81% Analysis Date = 04/21/18 Pct Recovery = 81% Analysis Date = 04/11/18 Pct Recovery = 80% Analysis Date = 04/11/18 Pct Recovery = 80% Analysis Date = 04/02/18 Pct Recovery = 80% Analysis Date = 04/02/18 Pct Recovery = 80% Analysis Date = 03/23/18 Pct Recovery = 80% Analysis Date = 03/23/18 Pct Recovery = 80% Analysis Date = 03/13/18 Pct Recovery = 80% Analysis Date = 03/13/18 Pct Recovery = 80% Analysis Date = 03/03/18 Pct Recovery = 80% Analysis Date = 03/03/18 Pct Recovery = 80% Analysis Date = 02/21/18 Pct Recovery = 79% Analysis Date = 02/21/18 Pct Recovery = 79% Analysis Date = 02/12/18 Pct Recovery = 79% Analysis Date = 02/12/18 Pct Recovery = 79% Analysis Date = 02/02/18 Pct Recovery = 79% Analysis Date = 02/02/18 Pct Recovery = 79% Analysis Date = 01/23/18 Pct Recovery = 79% Analysis Date = 01/23/18 Pct Recovery = 79% Analysis Date = 01/13/18 Pct Recovery = 78% Analysis Date = 01/13/18 Pct Recovery = 78% Analysis Date = 01/03/18 Pct Recovery = 78% Analysis Date = 01/03/18 Pct Recovery = 78% Analysis Date = 12/25/17 Pct Recovery = 78% Analysis Date = 12/25/17 Pct Recovery = 78% Analysis Date = 12/15/17 Pct Recovery = 78% Analysis Date = 12/15/17 Pct Recovery = 78% Analysis Date = 12/05/17 Pct Recovery = 78% Analysis Date = 12/05/17 Pct Recovery = 78% Analysis Date = 11/25/17 Pct Recovery = 77% Analysis Date = 11/25/17 Pct Recovery = 77% Analysis Date = 11/15/17 Pct Recovery = 77% Analysis Date = 11/15/17 Pct Recovery = 77% Analysis Date = 11/06/17 Pct Recovery = 77% Analysis Date = 11/06/17 Pct Recovery = 77% Analysis Date = 10/27/17 Pct Recovery = 77% Analysis Date = 10/27/17 Pct Recovery = 77% Analysis Date = 10/17/17 Pct Recovery = 77% Analysis Date = 10/17/17 Pct Recovery = 77% Analysis Date = 10/07/17 Pct Recovery = 76% Analysis Date = 10/07/17 Pct Recovery = 76% Analysis Date = 09/27/17 Pct Recovery = 76% Analysis Date = 09/27/17 Pct Recovery = 76% Analysis Date = 09/18/17 Pct Recovery = 76% Analysis Date = 09/18/17 Pct Recovery = 76% Analysis Date = 09/08/17 Pct Recovery = 76% Analysis Date = 09/08/17 Pct Recovery = 76% Analysis Date = 08/29/17 Pct Recovery = 75% Analysis Date = 08/29/17 Pct Recovery = 75% Analysis Date = 08/19/17 Pct Recovery = 75% Analysis Date = 08/19/17 Pct Recovery = 75% Analysis Date = 08/09/17 Pct Recovery = 75% Analysis Date = 08/09/17 Pct Recovery = 75% Analysis Date = 07/31/17 Pct Recovery = 75% Analysis Date = 07/31/17 Pct Recovery = 75% Analysis Date = 07/21/17 Pct Recovery = 75% Analysis Date = 07/21/17 Pct Recovery = 75% Analysis Date = 07/11/17 Pct Recovery = 74% Analysis Date = 07/11/17 Pct Recovery = 74% Analysis Date = 07/01/17 Pct Recovery = 74% Analysis Date = 07/01/17 Pct Recovery = 74% Analysis Date = 06/21/17 Pct Recovery = 74% Analysis Date = 06/21/17 Pct Recovery = 74% Analysis Date = 06/12/17 Pct Recovery = 74% Analysis Date = 06/12/17 Pct Recovery = 74% Analysis Date = 06/02/17 Pct Recovery = 74% Analysis Date = 06/02/17 Pct Recovery = 74% Analysis Date = 05/23/17 Pct Recovery = 73% Analysis Date = 05/23/17 Pct Recovery = 73% Analysis Date = 05/13/17 Pct Recovery = 73% Analysis Date = 05/13/17 Pct Recovery = 73% Analysis Date = 05/03/17 Pct Recovery = 73% Analysis Date = 05/03/17 Pct Recovery = 73% Analysis Date = 04/24/17 Pct Recovery = 73% Analysis Date = 04/24/17 Pct Recovery = 73% Analysis Date = 04/14/17 Pct Recovery = 73% Analysis Date = 04/14/17 Pct Recovery = 73% Analysis Date = 04/04/17 Pct Recovery = 72% Analysis Date = 04/04/17 Pct Recovery = 72% Analysis Date = 03/25/17 Pct Recovery = 72% Analysis Date = 03/25/17 Pct Recovery = 72% Analysis Date = 03/15/17 Pct Recovery = 72% Analysis Date = 03/15/17 Pct Recovery = 72% Analysis Date = 03/06/17 Pct Recovery = 72% Analysis Date = 03/06/17 Pct Recovery = 72% Analysis Date = 02/24/17 Pct Recovery = 71% Analysis Date = 02/24/17 Pct Recovery = 71% Analysis Date = 02/14/17 Pct Recovery = 71% Analysis Date = 02/14/17 Pct Recovery = 71% Analysis Date = 02/04/17 Pct Recovery = 71% Analysis Date = 02/04/17 Pct Recovery = 71% Analysis Date = 01/25/17 Pct Recovery = 71% Analysis Date = 01/25/17 Pct Recovery = 71% Analysis Date = 01/16/17 Pct Recovery = 71% Analysis Date = 01/16/17 Pct Recovery = 71% Analysis Date = 01/06/17 Pct Recovery = 70% Analysis Date = 01/06/17 Pct Recovery = 70% Analysis Date = 12/27/16 Pct Recovery = 70% Analysis Date = 12/27/16 Pct Recovery = 70% Analysis Date = 12/17/16 Pct Recovery = 70% Analysis Date = 12/17/16 Pct Recovery = 70% Analysis Date = 12/07/16 Pct Recovery = 70% Analysis Date = 12/07/16 Pct Recovery = 70% Analysis Date = 11/28/16 Pct Recovery = 69% Analysis Date = 11/28/16 Pct Recovery = 69% Analysis Date = 11/18/16 Pct Recovery = 69% Analysis Date = 11/18/16 Pct Recovery = 69% Analysis Date = 11/08/16 Pct Recovery = 69% Analysis Date = 11/08/16 Pct Recovery = 69% Analysis Date = 10/29/16 Pct Recovery = 69% Analysis Date = 10/29/16 Pct Recovery = 69% Analysis Date = 10/19/16 Pct Recovery = 69% Analysis Date = 10/19/16 Pct Recovery = 69% Analysis Date = 10/10/16 Pct Recovery = 68% Analysis Date = 10/10/16 Pct Recovery = 68% Analysis Date = 09/30/16 Pct Recovery = 68% Analysis Date = 09/30/16 Pct Recovery = 68% Analysis Date = 09/20/16 Pct Recovery = 68% Analysis Date = 09/20/16 Pct Recovery = 68% Analysis Date = 09/10/16 Pct Recovery = 68% Analysis Date = 09/10/16 Pct Recovery = 68% Analysis Date = 08/31/16 Pct Recovery = 67% Analysis Date = 08/31/16 Pct Recovery = 67% Analysis Date = 08/22/16 Pct Recovery = 67% Analysis Date = 08/22/16 Pct Recovery = 67% Analysis Date = 08/12/16 Pct Recovery = 67% Analysis Date = 08/12/16 Pct Recovery = 67% Analysis Date = 08/02/16 Pct Recovery = 67% Analysis Date = 08/02/16 Pct Recovery = 67% Analysis Date = 07/23/16 Pct Recovery = 67% Analysis Date = 07/23/16 Pct Recovery = 67% Analysis Date = 07/13/16 Pct Recovery = 67% Analysis Date = 07/13/16 Pct Recovery = 67% Analysis Date = 07/04/16 Pct Recovery = 67% Analysis Date = 07/04/16 Pct Recovery = 67% Analysis Date = 06/24/16 Pct Recovery = 66% Analysis Date = 06/24/16 Pct Recovery = 66% Analysis Date = 06/14/16 Pct Recovery = 66% Analysis Date = 06/14/16 Pct Recovery = 66% Analysis Date = 06/04/16 Pct Recovery = 66% Analysis Date = 06/04/16 Pct Recovery = 66% Analysis Date = 05/25/16 Pct Recovery = 66% Analysis Date = 05/25/16 Pct Recovery = 66% Analysis Date = 05/16/16 Pct Recovery = 66% Analysis Date = 05/16/16 Pct Recovery = 66% Analysis Date = 05/06/16 Pct Recovery = 66% Analysis Date = 05/06/16 Pct Recovery = 66% Analysis Date = 04/26/16 Pct Recovery = 66% Analysis Date = 04/26/16 Pct Recovery = 66% Analysis Date = 04/16/16 Pct Recovery = 66% Analysis Date = 04/16/16 Pct Recovery = 66% Analysis Date = 04/06/16 Pct Recovery = 65% Analysis Date = 04/06/16 Pct Recovery = 65% Analysis Date = 03/28/16 Pct Recovery = 65% Analysis Date = 03/28/16 Pct Recovery = 65% Analysis Date = 03/18/16 Pct Recovery = 65% Analysis Date = 03/18/16 Pct Recovery = 65% Analysis Date = 03/08/16 Pct Recovery = 65% Analysis Date = 03/08/16 Pct Recovery = 65% Analysis Date = 02/27/16 Pct Recovery = 65% Analysis Date = 02/27/16 Pct Recovery = 65% Analysis Date = 02/17/16 Pct Recovery = 65% Analysis Date = 02/17/16 Pct Recovery = 65% Analysis Date = 02/08/16 Pct Recovery = 65% Analysis Date = 02/08/16 Pct Recovery = 65% Analysis Date = 01/29/16 Pct Recovery = 65% Analysis Date = 01/29/16 Pct Recovery = 65% Analysis Date = 01/19/16 Pct Recovery = 65% Analysis Date = 01/19/16 Pct Recovery = 65% Analysis Date = 01/09/16 Pct Recovery = 64% Analysis Date = 01/09/16 Pct Recovery = 64% Analysis Date = 12/30/15 Pct Recovery = 64% Analysis Date = 12/30/15 Pct Recovery = 64% Analysis Date = 12/21/15 Pct Recovery = 64% Analysis Date = 12/21/15 Pct Recovery = 64% Analysis Date = 12/11/15 Pct Recovery = 64% Analysis Date = 12/11/15 Pct Recovery = 64% Analysis Date = 12/01/15 Pct Recovery = 64% Analysis Date = 12/01/15 Pct Recovery = 64% Analysis Date = 11/21/15 Pct Recovery = 64% Analysis Date = 11/21/15 Pct Recovery = 64% Analysis Date = 11/11/15 Pct Recovery = 64% Analysis Date = 11/11/15 Pct Recovery = 64% Analysis Date = 11/02/15 Pct Recovery = 64% Analysis Date = 11/02/15 Pct Recovery = 64% Analysis Date = 10/23/15 Pct Recovery = 64% Analysis Date = 10/23/15 Pct Recovery = 64% Analysis Date = 10/13/15 Pct Recovery = 63% Analysis Date = 10/13/15 Pct Recovery = 63% Analysis Date = 10/03/15 Pct Recovery = 63% Analysis Date = 10/03/15 Pct Recovery = 63% Analysis Date = 09/23/15 Pct Recovery = 63% Analysis Date = 09/23/15 Pct Recovery = 63% Analysis Date = 09/14/15 Pct Recovery = 63% Analysis Date = 09/14/15 Pct Recovery = 63% Analysis Date = 09/04/15 Pct Recovery = 63% Analysis Date = 09/04/15 Pct Recovery = 63% Analysis Date = 08/25/15 Pct Recovery = 63% Analysis Date = 08/25/15 Pct Recovery = 63% Analysis Date = 08/15/15 Pct Recovery = 63% Analysis Date = 08/15/15 Pct Recovery = 63% Analysis Date = 08/05/15 Pct Recovery = 63% Analysis Date = 08/05/15 Pct Recovery = 63% Analysis Date = 07/27/15 Pct Recovery = 63% Analysis Date = 07/27/15 Pct Recovery = 63% Analysis Date = 07/17/15 Pct Recovery = 62% Analysis Date = 07/17/15 Pct Recovery = 62% Analysis Date = 07/07/15 Pct Recovery = 62% Analysis Date = 07/07/15 Pct Recovery = 62% Analysis Date = 06/27/15 Pct Recovery = 62% Analysis Date = 06/27/15 Pct Recovery = 62% Analysis Date = 06/17/15 Pct Recovery = 62% Analysis Date = 06/17/15 Pct Recovery = 62% Analysis Date = 06/08/15 Pct Recovery = 62% Analysis Date = 06/08/15 Pct Recovery = 62% Analysis Date = 05/29/15 Pct Recovery = 62% Analysis Date = 05/29/15 Pct Recovery = 62% Analysis Date = 05/19/15 Pct Recovery = 62% Analysis Date = 05/19/15 Pct Recovery = 62% Analysis Date = 05/09/15 Pct Recovery = 62% Analysis Date = 05/09/15 Pct Recovery = 62% Analysis Date = 04/29/15 Pct Recovery = 62% Analysis Date = 04/29/15 Pct Recovery = 62% Analysis Date = 04/20/15 Pct Recovery = 62% Analysis Date = 04/20/15 Pct Recovery = 62% Analysis Date = 04/10/15 Pct Recovery = 62% Analysis Date = 04/10/15 Pct Recovery = 62% Analysis Date = 03/31/15 Pct Recovery = 62% Analysis Date = 03/31/15 Pct Recovery = 62% Analysis Date = 03/21/15 Pct Recovery = 62% Analysis Date = 03/21/15 Pct Recovery = 62% Analysis Date = 03/11/15 Pct Recovery = 62% Analysis Date = 03/11/15 Pct Recovery = 62% Analysis Date = 03/02/15 Pct Recovery = 63% Analysis Date = 03/02/15 Pct Recovery = 63% Analysis Date = 02/20/15 Pct Recovery = 63% Analysis Date = 02/20/15 Pct Recovery = 63% Analysis Date = 02/10/15 Pct Recovery = 63% Analysis Date = 02/10/15 Pct Recovery = 63% Analysis Date = 01/31/15 Pct Recovery = 63% Analysis Date = 01/31/15 Pct Recovery = 63% Analysis Date = 01/21/15 Pct Recovery = 63% Analysis Date = 01/21/15 Pct Recovery = 63% Analysis Date = 01/12/15 Pct Recovery = 63% Analysis Date = 01/12/15 Pct Recovery = 63% Analysis Date = 01/02/15 Pct Recovery = 63% Analysis Date = 01/02/15 Pct Recovery = 63% Analysis Date = 12/23/14 Pct Recovery = 63% Analysis Date = 12/23/14 Pct Recovery = 63% Analysis Date = 12/13/14 Pct Recovery = 63% Analysis Date = 12/13/14 Pct Recovery = 63% Analysis Date = 12/03/14 Pct Recovery = 63% Analysis Date = 12/03/14 Pct Recovery = 63% Analysis Date = 11/24/14 Pct Recovery = 63% Analysis Date = 11/24/14 Pct Recovery = 63% Analysis Date = 11/14/14 Pct Recovery = 63% Analysis Date = 11/14/14 Pct Recovery = 63% Analysis Date = 11/04/14 Pct Recovery = 64% Analysis Date = 11/04/14 Pct Recovery = 64% Analysis Date = 10/25/14 Pct Recovery = 64% Analysis Date = 10/25/14 Pct Recovery = 64% Analysis Date = 10/15/14 Pct Recovery = 64% Analysis Date = 10/15/14 Pct Recovery = 64% Analysis Date = 10/06/14 Pct Recovery = 64% Analysis Date = 10/06/14 Pct Recovery = 64% Analysis Date = 09/26/14 Pct Recovery = 64% Analysis Date = 09/26/14 Pct Recovery = 64% Analysis Date = 09/16/14 Pct Recovery = 64% Analysis Date = 09/16/14 Pct Recovery = 64% Analysis Date = 09/06/14 Pct Recovery = 65% Analysis Date = 09/06/14 Pct Recovery = 65% Analysis Date = 08/27/14 Pct Recovery = 65% Analysis Date = 08/27/14 Pct Recovery = 65% Analysis Date = 08/18/14 Pct Recovery = 65% Analysis Date = 08/18/14 Pct Recovery = 65% Analysis Date = 08/08/14 Pct Recovery = 65% Analysis Date = 08/08/14 Pct Recovery = 65% Analysis Date = 07/29/14 Pct Recovery = 66% Analysis Date = 07/29/14 Pct Recovery = 66% Analysis Date = 07/19/14 Pct Recovery = 66% Analysis Date = 07/19/14 Pct Recovery = 66% Analysis Date = 07/09/14 Pct Recovery = 66% Analysis Date = 07/09/14 Pct Recovery = 66% Analysis Date = 06/30/14 Pct Recovery = 66% Analysis Date = 06/30/14 Pct Recovery = 66% Analysis Date = 06/20/14 Pct Recovery = 67% Analysis Date = 06/20/14 Pct Recovery = 67% Analysis Date = 06/10/14 Pct Recovery = 67% Analysis Date = 06/10/14 Pct Recovery = 67% Analysis Date = 05/31/14 Pct Recovery = 67% Analysis Date = 05/31/14 Pct Recovery = 67% Analysis Date = 05/21/14 Pct Recovery = 67% Analysis Date = 05/21/14 Pct Recovery = 67% Analysis Date = 05/12/14 Pct Recovery = 68% Analysis Date = 05/12/14 Pct Recovery = 68% Analysis Date = 05/02/14 Pct Recovery = 68% Analysis Date = 05/02/14 Pct Recovery = 68% Analysis Date = 04/22/14 Pct Recovery = 68% Analysis Date = 04/22/14 Pct Recovery = 68% Analysis Date = 04/12/14 Pct Recovery = 69% Analysis Date = 04/12/14 Pct Recovery = 69% Analysis Date = 04/02/14 Pct Recovery = 69% Analysis Date = 04/02/14 Pct Recovery = 69% Analysis Date = 03/24/14 Pct Recovery = 69% Analysis Date = 03/24/14 Pct Recovery = 69% Analysis Date = 03/14/14 Pct Recovery = 69% Analysis Date = 03/14/14 Pct Recovery = 69% Analysis Date = 03/04/14 Pct Recovery = 70% Analysis Date = 03/04/14 Pct Recovery = 70% Analysis Date = 02/22/14 Pct Recovery = 70% Analysis Date = 02/22/14 Pct Recovery = 70% Analysis Date = 02/12/14 Pct Recovery = 70% Analysis Date = 02/12/14 Pct Recovery = 70% Analysis Date = 02/03/14 Pct Recovery = 71% Analysis Date = 02/03/14 Pct Recovery = 71% Analysis Date = 01/24/14 Pct Recovery = 71% Analysis Date = 01/24/14 Pct Recovery = 71% Analysis Date = 01/14/14 Pct Recovery = 71% Analysis Date = 01/14/14 Pct Recovery = 71% Analysis Date = 01/04/14 Pct Recovery = 71% Analysis Date = 01/04/14 Pct Recovery = 71% Analysis Date = 12/25/13 Pct Recovery = 72% Analysis Date = 12/25/13 Pct Recovery = 72% Analysis Date = 12/16/13 Pct Recovery = 72% Analysis Date = 12/16/13 Pct Recovery = 72% Analysis Date = 12/06/13 Pct Recovery = 72% Analysis Date = 12/06/13 Pct Recovery = 72% Analysis Date = 11/26/13 Pct Recovery = 73% Analysis Date = 11/26/13 Pct Recovery = 73% Analysis Date = 11/16/13 Pct Recovery = 73% Analysis Date = 11/16/13 Pct Recovery = 73% Analysis Date = 11/06/13 Pct Recovery = 73% Analysis Date = 11/06/13 Pct Recovery = 73% Analysis Date = 10/28/13 Pct Recovery = 74% Analysis Date = 10/28/13 Pct Recovery = 74% Analysis Date = 10/18/13 Pct Recovery = 74% Analysis Date = 10/18/13 Pct Recovery = 74% Analysis Date = 10/08/13 Pct Recovery = 74% Analysis Date = 10/08/13 Pct Recovery = 74% Analysis Date = 09/28/13 Pct Recovery = 75% Analysis Date = 09/28/13 Pct Recovery = 75% Analysis Date = 09/18/13 Pct Recovery = 75% Analysis Date = 09/18/13 Pct Recovery = 75% Analysis Date = 09/09/13 Pct Recovery = 75% Analysis Date = 09/09/13 Pct Recovery = 75% Analysis Date = 08/30/13 Pct Recovery = 76% Analysis Date = 08/30/13 Pct Recovery = 76% Analysis Date = 08/20/13 Pct Recovery = 76% Analysis Date = 08/20/13 Pct Recovery = 76% Analysis Date = 08/10/13 Pct Recovery = 76% Analysis Date = 08/10/13 Pct Recovery = 76% Analysis Date = 07/31/13 Pct Recovery = 77% Analysis Date = 07/31/13 Pct Recovery = 77% Analysis Date = 07/22/13 Pct Recovery = 77% Analysis Date = 07/22/13 Pct Recovery = 77% Analysis Date = 07/12/13 Pct Recovery = 77% Analysis Date = 07/12/13 Pct Recovery = 77% Analysis Date = 07/02/13 Pct Recovery = 78% Analysis Date = 07/02/13 Pct Recovery = 78% Analysis Date = 06/22/13 Pct Recovery = 78% Analysis Date = 06/22/13 Pct Recovery = 78% Analysis Date = 06/12/13 Pct Recovery = 78% Analysis Date = 06/12/13 Pct Recovery = 78% Analysis Date = 06/03/13 Pct Recovery = 79% Analysis Date = 06/03/13 Pct Recovery = 79% Analysis Date = 05/24/13 Pct Recovery = 79% Analysis Date = 05/24/13 Pct Recovery = 79% Analysis Date = 05/14/13 Pct Recovery = 79% Analysis Date = 05/14/13 Pct Recovery = 79% Analysis Date = 05/04/13 Pct Recovery = 80% Analysis Date = 05/04/13 Pct Recovery = 80% Analysis Date = 04/24/13 Pct Recovery = 80% Analysis Date = 04/24/13 Pct Recovery = 80% Analysis Date = 04/15/13 Pct Recovery = 80% Analysis Date = 04/15/13 Pct Recovery = 80% Analysis Date = 04/05/13 Pct Recovery = 81% Analysis Date = 04/05/13 Pct Recovery = 81% Analysis Date = 03/26/13 Pct Recovery = 81% Analysis Date = 03/26/13 Pct Recovery = 81% Analysis Date = 03/16/13 Pct Recovery = 81% Analysis Date = 03/16/13 Pct Recovery = 81% Analysis Date = 03/06/13 Pct Recovery = 82% Analysis Date = 03/06/13 Pct Recovery = 82% Analysis Date = 02/25/13 Pct Recovery = 82% Analysis Date = 02/25/13 Pct Recovery = 82% Analysis Date = 02/15/13 Pct Recovery = 82% Analysis Date = 02/15/13 Pct Recovery = 82% Analysis Date = 02/05/13 Pct Recovery = 83% Analysis Date = 02/05/13 Pct Recovery = 83% Analysis Date = 01/26/13 Pct Recovery = 83% Analysis Date = 01/26/13 Pct Recovery = 83% Analysis Date = 01/17/13 Pct Recovery = 83% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
AZINPHOS-METHYL

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 2 96% 4% 96% 4%
>= Reporting Level 81 69% 15% 66% 15%
Total 83 70% 16% 66% 16%

Sample Statistics
AZINPHOS-METHYL

Characteristic N % % Basis
Plotted 83 100% Spiked
Estimated Values 83 100% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 83 .  
False Negatives 0 0% 0 out of 83
Not Spiked 51 .  
False Positives 0 0% 0 out of 51

OBSP Determination:
AZINPHOS-METHYL-OXON
METHOD: 2033 , TESTIDCODE: 61635GCM39

Laboratory ID = 20130940097 Lab Value = 0.145 Expected Conc. = 0.5 Report level label = 0.042 Pct Recovery = 29% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = 0507-12-04.2 Laboratory ID = 20130250061 Lab Value = 0.318 Expected Conc. = 0.495 Report level label = 0.042 Pct Recovery = 64% Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl SpecificMix = 05BB029 Laboratory ID = 20140100085 Lab Value = 0.235 Expected Conc. = 0.352 Report level label = 0.042 Pct Recovery = 67% Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl SpecificMix = 042413 Laboratory ID = 20172510330 Lab Value = 0.182 Expected Conc. = 0.284 Report level label = 0.042 Pct Recovery = 64% Analysis Date = 12/29/17 SpikeMix = ChemService 6537100: 100 µl & Abs 071817Pest: 100 µl SpecificMix = 6537100 Laboratory ID = 20162860079 Lab Value = 0.167 Expected Conc. = 0.27 Report level label = 0.042 Pct Recovery = 62% Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl SpecificMix = 5054800 Laboratory ID = 20140230082 Lab Value = 0.161 Expected Conc. = 0.25 Report level label = 0.042 Pct Recovery = 64% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl SpecificMix = 012513 Laboratory ID = 20132420001 Lab Value = 0.140 Expected Conc. = 0.25 Report level label = 0.042 Pct Recovery = 56% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl SpecificMix = 012513 Laboratory ID = 20130100066 Lab Value = 0.219 Expected Conc. = 0.25 Report level label = 0.042 Pct Recovery = 88% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl SpecificMix = 052412 Laboratory ID = 20123560092 Lab Value = 0.157 Expected Conc. = 0.25 Report level label = 0.042 Pct Recovery = 63% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = 0507-12-04.2 Laboratory ID = 20171380001 Lab Value = 0.098 Expected Conc. = 0.216 Report level label = 0.042 Pct Recovery = 45% Analysis Date = 06/07/17 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 5054800 Laboratory ID = 20170960001 Lab Value = 0.149 Expected Conc. = 0.216 Report level label = 0.042 Pct Recovery = 69% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl SpecificMix = 5054800 Laboratory ID = 20161740258 Lab Value = 0.138 Expected Conc. = 0.216 Report level label = 0.042 Pct Recovery = 64% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 5054800 Laboratory ID = 20130510051 Lab Value = 0.131 Expected Conc. = 0.199 Report level label = 0.042 Pct Recovery = 66% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl SpecificMix = 0507-12-04.2 Laboratory ID = 20132690010 Lab Value = 0.112 Expected Conc. = 0.176 Report level label = 0.042 Pct Recovery = 64% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl SpecificMix = 042413 Laboratory ID = 20150720069 Lab Value = 0.045 Expected Conc. = 0.1698 Report level label = 0.042 Pct Recovery = 27% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 0227-14-08 Laboratory ID = 20141770149 Lab Value = 0.092 Expected Conc. = 0.1698 Report level label = 0.042 Pct Recovery = 54% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl SpecificMix = 0227-14-08 Laboratory ID = 20141570088 Lab Value = 0.086 Expected Conc. = 0.1698 Report level label = 0.042 Pct Recovery = 50% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl SpecificMix = 0227-14-08 Laboratory ID = 20172370001 Lab Value = 0.170 Expected Conc. = 0.142 Report level label = 0.042 Pct Recovery = 120% Analysis Date = 11/18/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6537100: 50 µl SpecificMix = 6537100 Laboratory ID = 20172230001 Lab Value = 0.109 Expected Conc. = 0.14 Report level label = 0.042 Pct Recovery = 78% Analysis Date = 10/19/17 SpikeMix = ChemService 6472100: 50 µl & Abs 071717Pest: 50 µl SpecificMix = 071717Pest Laboratory ID = 20152330039 Lab Value = 0.096 Expected Conc. = 0.126 Report level label = 0.042 Pct Recovery = 76% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl SpecificMix = 041415 Laboratory ID = 20151900132 Lab Value = 0.101 Expected Conc. = 0.126 Report level label = 0.042 Pct Recovery = 80% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl SpecificMix = 041415 Laboratory ID = 20151270112 Lab Value = 0.076 Expected Conc. = 0.126 Report level label = 0.042 Pct Recovery = 61% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl SpecificMix = 041415 Laboratory ID = 20172020035 Lab Value = 0.123 Expected Conc. = 0.112 Report level label = 0.042 Pct Recovery = 110% Analysis Date = 11/07/17 SpikeMix = Abs 071717Pest: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 071717Pest Laboratory ID = 20171940002 Lab Value = 0.114 Expected Conc. = 0.108 Report level label = 0.042 Pct Recovery = 106% Analysis Date = 11/10/17 SpikeMix = ChemService 5054800: 40 µl & NSI 041816: 40 µl SpecificMix = 5054800 Laboratory ID = 20170460061 Lab Value = 0.097 Expected Conc. = 0.108 Report level label = 0.042 Pct Recovery = 90% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl SpecificMix = 5054800 Laboratory ID = 20163560019 Lab Value = 0.075 Expected Conc. = 0.108 Report level label = 0.042 Pct Recovery = 69% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl SpecificMix = 5054800 Laboratory ID = 20140860102 Lab Value = 0.072 Expected Conc. = 0.1 Report level label = 0.042 Pct Recovery = 72% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 012513 Laboratory ID = 20133400002 Lab Value = 0.074 Expected Conc. = 0.1 Report level label = 0.042 Pct Recovery = 74% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = 052412 Laboratory ID = 20132910008 Lab Value = 0.040 Expected Conc. = 0.1 Report level label = 0.042 Pct Recovery = 40% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = 052412 Laboratory ID = 20131920149 Lab Value = 0.065 Expected Conc. = 0.1 Report level label = 0.042 Pct Recovery = 65% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl SpecificMix = 012513 Laboratory ID = 20130650005 Lab Value = 0.054 Expected Conc. = 0.1 Report level label = 0.042 Pct Recovery = 54% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl SpecificMix = 052412 Laboratory ID = 20131230084 Lab Value = 0.079 Expected Conc. = 0.099 Report level label = 0.042 Pct Recovery = 79% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl SpecificMix = 05BB029 Laboratory ID = 20173120093 Lab Value = 0.057 Expected Conc. = 0.0852 Report level label = 0.042 Pct Recovery = 67% Analysis Date = 03/10/18 SpikeMix = ChemService 6472100: 30 µl & ChemService 6537100: 30 µl SpecificMix = 6537100 Laboratory ID = 20172780018 Lab Value = 0.067 Expected Conc. = 0.0852 Report level label = 0.042 Pct Recovery = 79% Analysis Date = 02/08/18 SpikeMix = ChemService 6537100: 30 µl & Abs 071817Pest: 30 µl SpecificMix = 6537100 Laboratory ID = 20141490205 Lab Value = 0.060 Expected Conc. = 0.0849 Report level label = 0.042 Pct Recovery = 70% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20141420140 Lab Value = 0.033 Expected Conc. = 0.0849 Report level label = 0.042 Pct Recovery = 39% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20133580036 Lab Value = 0.057 Expected Conc. = 0.0704 Report level label = 0.042 Pct Recovery = 80% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 042413 Laboratory ID = 20133190012 Lab Value = 0.055 Expected Conc. = 0.0704 Report level label = 0.042 Pct Recovery = 78% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 042413 Laboratory ID = 20131650073 Lab Value = 0.064 Expected Conc. = 0.0704 Report level label = 0.042 Pct Recovery = 91% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl SpecificMix = 042413 Laboratory ID = 20133310030 Lab Value = 0.079 Expected Conc. = 0.0698 Report level label = 0.042 Pct Recovery = 113% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl SpecificMix = 04CC101 Laboratory ID = 20132280016 Lab Value = 0.064 Expected Conc. = 0.0698 Report level label = 0.042 Pct Recovery = 92% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl SpecificMix = 04CC101 Laboratory ID = 20131510026 Lab Value = 0.069 Expected Conc. = 0.0698 Report level label = 0.042 Pct Recovery = 99% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl SpecificMix = 04CC101 Laboratory ID = 20161050143 Lab Value = 0.064 Expected Conc. = 0.063 Report level label = 0.042 Pct Recovery = 102% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 041415 Laboratory ID = 20160560044 Lab Value = 0.071 Expected Conc. = 0.063 Report level label = 0.042 Pct Recovery = 113% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl SpecificMix = 041415 Laboratory ID = 20160210080 Lab Value = 0.041 Expected Conc. = 0.063 Report level label = 0.042 Pct Recovery = 65% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 041415 Laboratory ID = 20152950078 Lab Value = 0.039 Expected Conc. = 0.063 Report level label = 0.042 Pct Recovery = 62% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 041415 Laboratory ID = 20151210037 Lab Value = 0.034 Expected Conc. = 0.063 Report level label = 0.042 Pct Recovery = 54% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 041415 Analysis Date = 03/10/18 Pct Recovery = 85% Analysis Date = 02/28/18 Pct Recovery = 85% Analysis Date = 02/28/18 Pct Recovery = 85% Analysis Date = 02/19/18 Pct Recovery = 85% Analysis Date = 02/19/18 Pct Recovery = 85% Analysis Date = 02/09/18 Pct Recovery = 85% Analysis Date = 02/09/18 Pct Recovery = 85% Analysis Date = 01/31/18 Pct Recovery = 84% Analysis Date = 01/31/18 Pct Recovery = 84% Analysis Date = 01/22/18 Pct Recovery = 84% Analysis Date = 01/22/18 Pct Recovery = 84% Analysis Date = 01/12/18 Pct Recovery = 84% Analysis Date = 01/12/18 Pct Recovery = 84% Analysis Date = 01/03/18 Pct Recovery = 84% Analysis Date = 01/03/18 Pct Recovery = 84% Analysis Date = 12/24/17 Pct Recovery = 84% Analysis Date = 12/24/17 Pct Recovery = 84% Analysis Date = 12/15/17 Pct Recovery = 84% Analysis Date = 12/15/17 Pct Recovery = 84% Analysis Date = 12/06/17 Pct Recovery = 83% Analysis Date = 12/06/17 Pct Recovery = 83% Analysis Date = 11/26/17 Pct Recovery = 83% Analysis Date = 11/26/17 Pct Recovery = 83% Analysis Date = 11/17/17 Pct Recovery = 83% Analysis Date = 11/17/17 Pct Recovery = 83% Analysis Date = 11/07/17 Pct Recovery = 83% Analysis Date = 11/07/17 Pct Recovery = 83% Analysis Date = 10/29/17 Pct Recovery = 83% Analysis Date = 10/29/17 Pct Recovery = 83% Analysis Date = 10/20/17 Pct Recovery = 83% Analysis Date = 10/20/17 Pct Recovery = 83% Analysis Date = 10/10/17 Pct Recovery = 82% Analysis Date = 10/10/17 Pct Recovery = 82% Analysis Date = 10/01/17 Pct Recovery = 82% Analysis Date = 10/01/17 Pct Recovery = 82% Analysis Date = 09/21/17 Pct Recovery = 82% Analysis Date = 09/21/17 Pct Recovery = 82% Analysis Date = 09/12/17 Pct Recovery = 82% Analysis Date = 09/12/17 Pct Recovery = 82% Analysis Date = 09/03/17 Pct Recovery = 82% Analysis Date = 09/03/17 Pct Recovery = 82% Analysis Date = 08/24/17 Pct Recovery = 82% Analysis Date = 08/24/17 Pct Recovery = 82% Analysis Date = 08/15/17 Pct Recovery = 82% Analysis Date = 08/15/17 Pct Recovery = 82% Analysis Date = 08/05/17 Pct Recovery = 81% Analysis Date = 08/05/17 Pct Recovery = 81% Analysis Date = 07/27/17 Pct Recovery = 81% Analysis Date = 07/27/17 Pct Recovery = 81% Analysis Date = 07/18/17 Pct Recovery = 81% Analysis Date = 07/18/17 Pct Recovery = 81% Analysis Date = 07/08/17 Pct Recovery = 81% Analysis Date = 07/08/17 Pct Recovery = 81% Analysis Date = 06/29/17 Pct Recovery = 81% Analysis Date = 06/29/17 Pct Recovery = 81% Analysis Date = 06/19/17 Pct Recovery = 81% Analysis Date = 06/19/17 Pct Recovery = 81% Analysis Date = 06/10/17 Pct Recovery = 80% Analysis Date = 06/10/17 Pct Recovery = 80% Analysis Date = 06/01/17 Pct Recovery = 80% Analysis Date = 06/01/17 Pct Recovery = 80% Analysis Date = 05/22/17 Pct Recovery = 80% Analysis Date = 05/22/17 Pct Recovery = 80% Analysis Date = 05/13/17 Pct Recovery = 80% Analysis Date = 05/13/17 Pct Recovery = 80% Analysis Date = 05/03/17 Pct Recovery = 80% Analysis Date = 05/03/17 Pct Recovery = 80% Analysis Date = 04/24/17 Pct Recovery = 80% Analysis Date = 04/24/17 Pct Recovery = 80% Analysis Date = 04/15/17 Pct Recovery = 79% Analysis Date = 04/15/17 Pct Recovery = 79% Analysis Date = 04/05/17 Pct Recovery = 79% Analysis Date = 04/05/17 Pct Recovery = 79% Analysis Date = 03/27/17 Pct Recovery = 79% Analysis Date = 03/27/17 Pct Recovery = 79% Analysis Date = 03/17/17 Pct Recovery = 79% Analysis Date = 03/17/17 Pct Recovery = 79% Analysis Date = 03/08/17 Pct Recovery = 79% Analysis Date = 03/08/17 Pct Recovery = 79% Analysis Date = 02/27/17 Pct Recovery = 79% Analysis Date = 02/27/17 Pct Recovery = 79% Analysis Date = 02/17/17 Pct Recovery = 78% Analysis Date = 02/17/17 Pct Recovery = 78% Analysis Date = 02/08/17 Pct Recovery = 78% Analysis Date = 02/08/17 Pct Recovery = 78% Analysis Date = 01/29/17 Pct Recovery = 78% Analysis Date = 01/29/17 Pct Recovery = 78% Analysis Date = 01/20/17 Pct Recovery = 78% Analysis Date = 01/20/17 Pct Recovery = 78% Analysis Date = 01/11/17 Pct Recovery = 78% Analysis Date = 01/11/17 Pct Recovery = 78% Analysis Date = 01/01/17 Pct Recovery = 77% Analysis Date = 01/01/17 Pct Recovery = 77% Analysis Date = 12/23/16 Pct Recovery = 77% Analysis Date = 12/23/16 Pct Recovery = 77% Analysis Date = 12/13/16 Pct Recovery = 77% Analysis Date = 12/13/16 Pct Recovery = 77% Analysis Date = 12/04/16 Pct Recovery = 77% Analysis Date = 12/04/16 Pct Recovery = 77% Analysis Date = 11/25/16 Pct Recovery = 77% Analysis Date = 11/25/16 Pct Recovery = 77% Analysis Date = 11/15/16 Pct Recovery = 76% Analysis Date = 11/15/16 Pct Recovery = 76% Analysis Date = 11/06/16 Pct Recovery = 76% Analysis Date = 11/06/16 Pct Recovery = 76% Analysis Date = 10/27/16 Pct Recovery = 76% Analysis Date = 10/27/16 Pct Recovery = 76% Analysis Date = 10/18/16 Pct Recovery = 76% Analysis Date = 10/18/16 Pct Recovery = 76% Analysis Date = 10/09/16 Pct Recovery = 75% Analysis Date = 10/09/16 Pct Recovery = 75% Analysis Date = 09/29/16 Pct Recovery = 75% Analysis Date = 09/29/16 Pct Recovery = 75% Analysis Date = 09/20/16 Pct Recovery = 75% Analysis Date = 09/20/16 Pct Recovery = 75% Analysis Date = 09/10/16 Pct Recovery = 75% Analysis Date = 09/10/16 Pct Recovery = 75% Analysis Date = 09/01/16 Pct Recovery = 75% Analysis Date = 09/01/16 Pct Recovery = 75% Analysis Date = 08/23/16 Pct Recovery = 74% Analysis Date = 08/23/16 Pct Recovery = 74% Analysis Date = 08/13/16 Pct Recovery = 74% Analysis Date = 08/13/16 Pct Recovery = 74% Analysis Date = 08/04/16 Pct Recovery = 74% Analysis Date = 08/04/16 Pct Recovery = 74% Analysis Date = 07/25/16 Pct Recovery = 74% Analysis Date = 07/25/16 Pct Recovery = 74% Analysis Date = 07/16/16 Pct Recovery = 74% Analysis Date = 07/16/16 Pct Recovery = 74% Analysis Date = 07/07/16 Pct Recovery = 73% Analysis Date = 07/07/16 Pct Recovery = 73% Analysis Date = 06/27/16 Pct Recovery = 73% Analysis Date = 06/27/16 Pct Recovery = 73% Analysis Date = 06/18/16 Pct Recovery = 73% Analysis Date = 06/18/16 Pct Recovery = 73% Analysis Date = 06/08/16 Pct Recovery = 73% Analysis Date = 06/08/16 Pct Recovery = 73% Analysis Date = 05/30/16 Pct Recovery = 73% Analysis Date = 05/30/16 Pct Recovery = 73% Analysis Date = 05/21/16 Pct Recovery = 72% Analysis Date = 05/21/16 Pct Recovery = 72% Analysis Date = 05/11/16 Pct Recovery = 72% Analysis Date = 05/11/16 Pct Recovery = 72% Analysis Date = 05/02/16 Pct Recovery = 72% Analysis Date = 05/02/16 Pct Recovery = 72% Analysis Date = 04/22/16 Pct Recovery = 72% Analysis Date = 04/22/16 Pct Recovery = 72% Analysis Date = 04/13/16 Pct Recovery = 72% Analysis Date = 04/13/16 Pct Recovery = 72% Analysis Date = 04/04/16 Pct Recovery = 71% Analysis Date = 04/04/16 Pct Recovery = 71% Analysis Date = 03/25/16 Pct Recovery = 71% Analysis Date = 03/25/16 Pct Recovery = 71% Analysis Date = 03/16/16 Pct Recovery = 71% Analysis Date = 03/16/16 Pct Recovery = 71% Analysis Date = 03/06/16 Pct Recovery = 71% Analysis Date = 03/06/16 Pct Recovery = 71% Analysis Date = 02/26/16 Pct Recovery = 71% Analysis Date = 02/26/16 Pct Recovery = 71% Analysis Date = 02/17/16 Pct Recovery = 71% Analysis Date = 02/17/16 Pct Recovery = 71% Analysis Date = 02/07/16 Pct Recovery = 71% Analysis Date = 02/07/16 Pct Recovery = 71% Analysis Date = 01/29/16 Pct Recovery = 70% Analysis Date = 01/29/16 Pct Recovery = 70% Analysis Date = 01/19/16 Pct Recovery = 70% Analysis Date = 01/19/16 Pct Recovery = 70% Analysis Date = 01/10/16 Pct Recovery = 70% Analysis Date = 01/10/16 Pct Recovery = 70% Analysis Date = 01/01/16 Pct Recovery = 70% Analysis Date = 01/01/16 Pct Recovery = 70% Analysis Date = 12/22/15 Pct Recovery = 70% Analysis Date = 12/22/15 Pct Recovery = 70% Analysis Date = 12/13/15 Pct Recovery = 70% Analysis Date = 12/13/15 Pct Recovery = 70% Analysis Date = 12/03/15 Pct Recovery = 70% Analysis Date = 12/03/15 Pct Recovery = 70% Analysis Date = 11/24/15 Pct Recovery = 70% Analysis Date = 11/24/15 Pct Recovery = 70% Analysis Date = 11/15/15 Pct Recovery = 69% Analysis Date = 11/15/15 Pct Recovery = 69% Analysis Date = 11/05/15 Pct Recovery = 69% Analysis Date = 11/05/15 Pct Recovery = 69% Analysis Date = 10/27/15 Pct Recovery = 69% Analysis Date = 10/27/15 Pct Recovery = 69% Analysis Date = 10/17/15 Pct Recovery = 69% Analysis Date = 10/17/15 Pct Recovery = 69% Analysis Date = 10/08/15 Pct Recovery = 69% Analysis Date = 10/08/15 Pct Recovery = 69% Analysis Date = 09/29/15 Pct Recovery = 69% Analysis Date = 09/29/15 Pct Recovery = 69% Analysis Date = 09/19/15 Pct Recovery = 69% Analysis Date = 09/19/15 Pct Recovery = 69% Analysis Date = 09/10/15 Pct Recovery = 68% Analysis Date = 09/10/15 Pct Recovery = 68% Analysis Date = 08/31/15 Pct Recovery = 68% Analysis Date = 08/31/15 Pct Recovery = 68% Analysis Date = 08/22/15 Pct Recovery = 68% Analysis Date = 08/22/15 Pct Recovery = 68% Analysis Date = 08/13/15 Pct Recovery = 68% Analysis Date = 08/13/15 Pct Recovery = 68% Analysis Date = 08/03/15 Pct Recovery = 68% Analysis Date = 08/03/15 Pct Recovery = 68% Analysis Date = 07/25/15 Pct Recovery = 68% Analysis Date = 07/25/15 Pct Recovery = 68% Analysis Date = 07/15/15 Pct Recovery = 68% Analysis Date = 07/15/15 Pct Recovery = 68% Analysis Date = 07/06/15 Pct Recovery = 67% Analysis Date = 07/06/15 Pct Recovery = 67% Analysis Date = 06/27/15 Pct Recovery = 67% Analysis Date = 06/27/15 Pct Recovery = 67% Analysis Date = 06/17/15 Pct Recovery = 67% Analysis Date = 06/17/15 Pct Recovery = 67% Analysis Date = 06/08/15 Pct Recovery = 67% Analysis Date = 06/08/15 Pct Recovery = 67% Analysis Date = 05/29/15 Pct Recovery = 67% Analysis Date = 05/29/15 Pct Recovery = 67% Analysis Date = 05/20/15 Pct Recovery = 67% Analysis Date = 05/20/15 Pct Recovery = 67% Analysis Date = 05/11/15 Pct Recovery = 67% Analysis Date = 05/11/15 Pct Recovery = 67% Analysis Date = 05/01/15 Pct Recovery = 66% Analysis Date = 05/01/15 Pct Recovery = 66% Analysis Date = 04/22/15 Pct Recovery = 66% Analysis Date = 04/22/15 Pct Recovery = 66% Analysis Date = 04/12/15 Pct Recovery = 66% Analysis Date = 04/12/15 Pct Recovery = 66% Analysis Date = 04/03/15 Pct Recovery = 66% Analysis Date = 04/03/15 Pct Recovery = 66% Analysis Date = 03/25/15 Pct Recovery = 66% Analysis Date = 03/25/15 Pct Recovery = 66% Analysis Date = 03/15/15 Pct Recovery = 66% Analysis Date = 03/15/15 Pct Recovery = 66% Analysis Date = 03/06/15 Pct Recovery = 65% Analysis Date = 03/06/15 Pct Recovery = 65% Analysis Date = 02/24/15 Pct Recovery = 65% Analysis Date = 02/24/15 Pct Recovery = 65% Analysis Date = 02/15/15 Pct Recovery = 65% Analysis Date = 02/15/15 Pct Recovery = 65% Analysis Date = 02/06/15 Pct Recovery = 65% Analysis Date = 02/06/15 Pct Recovery = 65% Analysis Date = 01/27/15 Pct Recovery = 65% Analysis Date = 01/27/15 Pct Recovery = 65% Analysis Date = 01/18/15 Pct Recovery = 65% Analysis Date = 01/18/15 Pct Recovery = 65% Analysis Date = 01/08/15 Pct Recovery = 64% Analysis Date = 01/08/15 Pct Recovery = 64% Analysis Date = 12/30/14 Pct Recovery = 64% Analysis Date = 12/30/14 Pct Recovery = 64% Analysis Date = 12/21/14 Pct Recovery = 64% Analysis Date = 12/21/14 Pct Recovery = 64% Analysis Date = 12/11/14 Pct Recovery = 64% Analysis Date = 12/11/14 Pct Recovery = 64% Analysis Date = 12/02/14 Pct Recovery = 64% Analysis Date = 12/02/14 Pct Recovery = 64% Analysis Date = 11/22/14 Pct Recovery = 64% Analysis Date = 11/22/14 Pct Recovery = 64% Analysis Date = 11/13/14 Pct Recovery = 63% Analysis Date = 11/13/14 Pct Recovery = 63% Analysis Date = 11/04/14 Pct Recovery = 63% Analysis Date = 11/04/14 Pct Recovery = 63% Analysis Date = 10/25/14 Pct Recovery = 63% Analysis Date = 10/25/14 Pct Recovery = 63% Analysis Date = 10/16/14 Pct Recovery = 63% Analysis Date = 10/16/14 Pct Recovery = 63% Analysis Date = 10/06/14 Pct Recovery = 63% Analysis Date = 10/06/14 Pct Recovery = 63% Analysis Date = 09/27/14 Pct Recovery = 63% Analysis Date = 09/27/14 Pct Recovery = 63% Analysis Date = 09/18/14 Pct Recovery = 62% Analysis Date = 09/18/14 Pct Recovery = 62% Analysis Date = 09/08/14 Pct Recovery = 62% Analysis Date = 09/08/14 Pct Recovery = 62% Analysis Date = 08/30/14 Pct Recovery = 62% Analysis Date = 08/30/14 Pct Recovery = 62% Analysis Date = 08/20/14 Pct Recovery = 62% Analysis Date = 08/20/14 Pct Recovery = 62% Analysis Date = 08/11/14 Pct Recovery = 62% Analysis Date = 08/11/14 Pct Recovery = 62% Analysis Date = 08/02/14 Pct Recovery = 62% Analysis Date = 08/02/14 Pct Recovery = 62% Analysis Date = 07/23/14 Pct Recovery = 61% Analysis Date = 07/23/14 Pct Recovery = 61% Analysis Date = 07/14/14 Pct Recovery = 61% Analysis Date = 07/14/14 Pct Recovery = 61% Analysis Date = 07/04/14 Pct Recovery = 61% Analysis Date = 07/04/14 Pct Recovery = 61% Analysis Date = 06/25/14 Pct Recovery = 61% Analysis Date = 06/25/14 Pct Recovery = 61% Analysis Date = 06/16/14 Pct Recovery = 61% Analysis Date = 06/16/14 Pct Recovery = 61% Analysis Date = 06/06/14 Pct Recovery = 62% Analysis Date = 06/06/14 Pct Recovery = 62% Analysis Date = 05/28/14 Pct Recovery = 62% Analysis Date = 05/28/14 Pct Recovery = 62% Analysis Date = 05/18/14 Pct Recovery = 62% Analysis Date = 05/18/14 Pct Recovery = 62% Analysis Date = 05/09/14 Pct Recovery = 62% Analysis Date = 05/09/14 Pct Recovery = 62% Analysis Date = 04/30/14 Pct Recovery = 63% Analysis Date = 04/30/14 Pct Recovery = 63% Analysis Date = 04/20/14 Pct Recovery = 63% Analysis Date = 04/20/14 Pct Recovery = 63% Analysis Date = 04/11/14 Pct Recovery = 63% Analysis Date = 04/11/14 Pct Recovery = 63% Analysis Date = 04/01/14 Pct Recovery = 64% Analysis Date = 04/01/14 Pct Recovery = 64% Analysis Date = 03/23/14 Pct Recovery = 64% Analysis Date = 03/23/14 Pct Recovery = 64% Analysis Date = 03/14/14 Pct Recovery = 65% Analysis Date = 03/14/14 Pct Recovery = 65% Analysis Date = 03/04/14 Pct Recovery = 65% Analysis Date = 03/04/14 Pct Recovery = 65% Analysis Date = 02/23/14 Pct Recovery = 65% Analysis Date = 02/23/14 Pct Recovery = 65% Analysis Date = 02/13/14 Pct Recovery = 66% Analysis Date = 02/13/14 Pct Recovery = 66% Analysis Date = 02/04/14 Pct Recovery = 66% Analysis Date = 02/04/14 Pct Recovery = 66% Analysis Date = 01/26/14 Pct Recovery = 67% Analysis Date = 01/26/14 Pct Recovery = 67% Analysis Date = 01/16/14 Pct Recovery = 67% Analysis Date = 01/16/14 Pct Recovery = 67% Analysis Date = 01/07/14 Pct Recovery = 68% Analysis Date = 01/07/14 Pct Recovery = 68% Analysis Date = 12/28/13 Pct Recovery = 68% Analysis Date = 12/28/13 Pct Recovery = 68% Analysis Date = 12/19/13 Pct Recovery = 68% Analysis Date = 12/19/13 Pct Recovery = 68% Analysis Date = 12/10/13 Pct Recovery = 68% Analysis Date = 12/10/13 Pct Recovery = 68% Analysis Date = 11/30/13 Pct Recovery = 68% Analysis Date = 11/30/13 Pct Recovery = 68% Analysis Date = 11/21/13 Pct Recovery = 68% Analysis Date = 11/21/13 Pct Recovery = 68% Analysis Date = 11/11/13 Pct Recovery = 69% Analysis Date = 11/11/13 Pct Recovery = 69% Analysis Date = 11/02/13 Pct Recovery = 69% Analysis Date = 11/02/13 Pct Recovery = 69% Analysis Date = 10/24/13 Pct Recovery = 69% Analysis Date = 10/24/13 Pct Recovery = 69% Analysis Date = 10/14/13 Pct Recovery = 69% Analysis Date = 10/14/13 Pct Recovery = 69% Analysis Date = 10/05/13 Pct Recovery = 69% Analysis Date = 10/05/13 Pct Recovery = 69% Analysis Date = 09/25/13 Pct Recovery = 69% Analysis Date = 09/25/13 Pct Recovery = 69% Analysis Date = 09/16/13 Pct Recovery = 69% Analysis Date = 09/16/13 Pct Recovery = 69% Analysis Date = 09/07/13 Pct Recovery = 69% Analysis Date = 09/07/13 Pct Recovery = 69% Analysis Date = 08/28/13 Pct Recovery = 70% Analysis Date = 08/28/13 Pct Recovery = 70% Analysis Date = 08/19/13 Pct Recovery = 70% Analysis Date = 08/19/13 Pct Recovery = 70% Analysis Date = 08/09/13 Pct Recovery = 70% Analysis Date = 08/09/13 Pct Recovery = 70% Analysis Date = 07/31/13 Pct Recovery = 70% Analysis Date = 07/31/13 Pct Recovery = 70% Analysis Date = 07/22/13 Pct Recovery = 70% Analysis Date = 07/22/13 Pct Recovery = 70% Analysis Date = 07/12/13 Pct Recovery = 70% Analysis Date = 07/12/13 Pct Recovery = 70% Analysis Date = 07/03/13 Pct Recovery = 70% Analysis Date = 07/03/13 Pct Recovery = 70% Analysis Date = 06/23/13 Pct Recovery = 70% Analysis Date = 06/23/13 Pct Recovery = 70% Analysis Date = 06/14/13 Pct Recovery = 70% Analysis Date = 06/14/13 Pct Recovery = 70% Analysis Date = 06/05/13 Pct Recovery = 70% Analysis Date = 06/05/13 Pct Recovery = 70% Analysis Date = 05/26/13 Pct Recovery = 70% Analysis Date = 05/26/13 Pct Recovery = 70% Analysis Date = 05/17/13 Pct Recovery = 70% Analysis Date = 05/17/13 Pct Recovery = 70% Analysis Date = 05/07/13 Pct Recovery = 70% Analysis Date = 05/07/13 Pct Recovery = 70% Analysis Date = 04/28/13 Pct Recovery = 71% Analysis Date = 04/28/13 Pct Recovery = 71% Analysis Date = 04/19/13 Pct Recovery = 71% Analysis Date = 04/19/13 Pct Recovery = 71% Analysis Date = 04/09/13 Pct Recovery = 71% Analysis Date = 04/09/13 Pct Recovery = 71% Analysis Date = 03/31/13 Pct Recovery = 71% Analysis Date = 03/31/13 Pct Recovery = 71% Analysis Date = 03/21/13 Pct Recovery = 71% Analysis Date = 03/21/13 Pct Recovery = 71% Analysis Date = 03/12/13 Pct Recovery = 71% Analysis Date = 03/12/13 Pct Recovery = 71% Analysis Date = 03/03/13 Pct Recovery = 71% Analysis Date = 03/03/13 Pct Recovery = 71% Analysis Date = 02/21/13 Pct Recovery = 71% Analysis Date = 02/21/13 Pct Recovery = 71% Analysis Date = 02/12/13 Pct Recovery = 71% Analysis Date = 02/12/13 Pct Recovery = 71% Analysis Date = 02/02/13 Pct Recovery = 71% Analysis Date = 02/02/13 Pct Recovery = 71% Analysis Date = 01/24/13 Pct Recovery = 71% Analysis Date = 01/24/13 Pct Recovery = 71% Analysis Date = 01/15/13 Pct Recovery = 71% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
AZINPHOS-METHYL-OXON

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 47 72% 21% 67% 14%
Total 47 72% 21% 67% 14%

Sample Statistics
AZINPHOS-METHYL-OXON

Characteristic N % % Basis
Plotted 47 84% Spiked
Estimated Values 47 84% Spiked
Deleted Values 2 2% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 56 .  
False Negatives 9 16% 9 out of 56
Not Spiked 62 .  
False Positives 2 3% 2 out of 60

OBSP Determination:
BENFLURALIN
METHOD: 2033 , TESTIDCODE: 82673GCM35

Laboratory ID = 20132490342 Lab Value = 0.088 Expected Conc. = 0.149 Report level label = 0.014 Pct Recovery = 59% Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20172510330 Lab Value = 0.057 Expected Conc. = 0.094 Report level label = 0.014 Pct Recovery = 60% Analysis Date = 12/29/17 SpikeMix = ChemService 6537100: 100 µl & Abs 071817Pest: 100 µl SpecificMix = 071817Pest Laboratory ID = 20162860079 Lab Value = 0.070 Expected Conc. = 0.088 Report level label = 0.014 Pct Recovery = 80% Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl SpecificMix = 060916 Laboratory ID = 20163150006 Lab Value = 0.064 Expected Conc. = 0.088 Report level label = 0.014 Pct Recovery = 73% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl SpecificMix = 060916 Laboratory ID = 20152610011 Lab Value = 0.056 Expected Conc. = 0.084 Report level label = 0.014 Pct Recovery = 66% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl SpecificMix = 0406-15-01 Laboratory ID = 20152460215 Lab Value = 0.048 Expected Conc. = 0.084 Report level label = 0.014 Pct Recovery = 58% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl SpecificMix = 0406-15-01 Laboratory ID = 20132140002 Lab Value = 0.057 Expected Conc. = 0.0752 Report level label = 0.014 Pct Recovery = 76% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl SpecificMix = LB99392 Laboratory ID = 20131370001 Lab Value = 0.060 Expected Conc. = 0.0752 Report level label = 0.014 Pct Recovery = 79% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl SpecificMix = LB99392 Laboratory ID = 20140370077 Lab Value = 0.038 Expected Conc. = 0.0745 Report level label = 0.014 Pct Recovery = 51% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20132560001 Lab Value = 0.064 Expected Conc. = 0.0745 Report level label = 0.014 Pct Recovery = 86% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20171380001 Lab Value = 0.043 Expected Conc. = 0.0712 Report level label = 0.014 Pct Recovery = 60% Analysis Date = 06/07/17 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 041816 Laboratory ID = 20170740063 Lab Value = 0.056 Expected Conc. = 0.0712 Report level label = 0.014 Pct Recovery = 78% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl SpecificMix = 041816 Laboratory ID = 20161740258 Lab Value = 0.040 Expected Conc. = 0.0712 Report level label = 0.014 Pct Recovery = 56% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 041816 Laboratory ID = 20171660002 Lab Value = 0.051 Expected Conc. = 0.0704 Report level label = 0.014 Pct Recovery = 72% Analysis Date = 08/23/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = 060916 Laboratory ID = 20170190026 Lab Value = 0.050 Expected Conc. = 0.0704 Report level label = 0.014 Pct Recovery = 72% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = 060916 Laboratory ID = 20150430092 Lab Value = 0.040 Expected Conc. = 0.0559 Report level label = 0.014 Pct Recovery = 72% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl SpecificMix = E1140407002 Laboratory ID = 20143110108 Lab Value = 0.037 Expected Conc. = 0.0559 Report level label = 0.014 Pct Recovery = 66% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl SpecificMix = E1140407002 Laboratory ID = 20142720002 Lab Value = 0.034 Expected Conc. = 0.0559 Report level label = 0.014 Pct Recovery = 60% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl SpecificMix = E1140407002 Laboratory ID = 20141770149 Lab Value = 0.038 Expected Conc. = 0.0559 Report level label = 0.014 Pct Recovery = 69% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl SpecificMix = E1140407002 Laboratory ID = 20143240095 Lab Value = 0.049 Expected Conc. = 0.0558 Report level label = 0.014 Pct Recovery = 87% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl SpecificMix = 032714 Laboratory ID = 20142270001 Lab Value = 0.030 Expected Conc. = 0.0558 Report level label = 0.014 Pct Recovery = 53% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl SpecificMix = 032714 Laboratory ID = 20141220025 Lab Value = 0.043 Expected Conc. = 0.0558 Report level label = 0.014 Pct Recovery = 77% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl SpecificMix = 032714 Laboratory ID = 20172560101 Lab Value = 0.029 Expected Conc. = 0.05 Report level label = 0.014 Pct Recovery = 58% Analysis Date = 12/22/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6567600: 50 µl SpecificMix = 6567600 Laboratory ID = 20130940097 Lab Value = 0.038 Expected Conc. = 0.05 Report level label = 0.014 Pct Recovery = 76% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = 0507-12-04.2 Laboratory ID = 20130810108 Lab Value = 0.032 Expected Conc. = 0.05 Report level label = 0.014 Pct Recovery = 64% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl SpecificMix = LB92783 Laboratory ID = 20130100066 Lab Value = 0.043 Expected Conc. = 0.05 Report level label = 0.014 Pct Recovery = 86% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl SpecificMix = LB92783 Laboratory ID = 20123560092 Lab Value = 0.033 Expected Conc. = 0.05 Report level label = 0.014 Pct Recovery = 66% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = 0507-12-04.2 Laboratory ID = 20181430122 Lab Value = 0.046 Expected Conc. = 0.047 Report level label = 0.014 Pct Recovery = 97% Analysis Date = 06/20/18 SpikeMix = Abs 071817Pest: 50 µl & Spex Organics EN170808006: 50 µl SpecificMix = 071817Pest Laboratory ID = 20161260151 Lab Value = 0.028 Expected Conc. = 0.044 Report level label = 0.014 Pct Recovery = 64% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = 3851600 Laboratory ID = 20151550293 Lab Value = 0.031 Expected Conc. = 0.044 Report level label = 0.014 Pct Recovery = 71% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl SpecificMix = 3851600 Laboratory ID = 20151270112 Lab Value = 0.027 Expected Conc. = 0.044 Report level label = 0.014 Pct Recovery = 61% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl SpecificMix = 3851600 Laboratory ID = 20160770090 Lab Value = 0.027 Expected Conc. = 0.042 Report level label = 0.014 Pct Recovery = 64% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20160630046 Lab Value = 0.026 Expected Conc. = 0.042 Report level label = 0.014 Pct Recovery = 62% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20153510109 Lab Value = 0.028 Expected Conc. = 0.042 Report level label = 0.014 Pct Recovery = 67% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20153440001 Lab Value = 0.028 Expected Conc. = 0.042 Report level label = 0.014 Pct Recovery = 68% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20171940002 Lab Value = 0.029 Expected Conc. = 0.0356 Report level label = 0.014 Pct Recovery = 82% Analysis Date = 11/10/17 SpikeMix = ChemService 5054800: 40 µl & NSI 041816: 40 µl SpecificMix = 041816 Laboratory ID = 20162020124 Lab Value = 0.024 Expected Conc. = 0.0356 Report level label = 0.014 Pct Recovery = 68% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl SpecificMix = 041816 Laboratory ID = 20161600087 Lab Value = 0.026 Expected Conc. = 0.0356 Report level label = 0.014 Pct Recovery = 73% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 041816 Laboratory ID = 20161340228 Lab Value = 0.024 Expected Conc. = 0.0356 Report level label = 0.014 Pct Recovery = 68% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl SpecificMix = 041816 Laboratory ID = 20161190075 Lab Value = 0.023 Expected Conc. = 0.0356 Report level label = 0.014 Pct Recovery = 66% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 041816 Laboratory ID = 20171160110 Lab Value = 0.026 Expected Conc. = 0.0352 Report level label = 0.014 Pct Recovery = 74% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = 060916 Laboratory ID = 20162520001 Lab Value = 0.037 Expected Conc. = 0.0352 Report level label = 0.014 Pct Recovery = 105% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl SpecificMix = 060916 Laboratory ID = 20163560019 Lab Value = 0.030 Expected Conc. = 0.0352 Report level label = 0.014 Pct Recovery = 85% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl SpecificMix = 060916 Laboratory ID = 20162380004 Lab Value = 0.025 Expected Conc. = 0.0352 Report level label = 0.014 Pct Recovery = 72% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = 060916 Laboratory ID = 20140510043 Lab Value = 0.026 Expected Conc. = 0.0301 Report level label = 0.014 Pct Recovery = 87% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl SpecificMix = LB99392 Laboratory ID = 20133470008 Lab Value = 0.022 Expected Conc. = 0.0301 Report level label = 0.014 Pct Recovery = 73% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl SpecificMix = LB99392 Laboratory ID = 20133190012 Lab Value = 0.033 Expected Conc. = 0.0301 Report level label = 0.014 Pct Recovery = 111% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = LB99392 Laboratory ID = 20133050050 Lab Value = 0.026 Expected Conc. = 0.0301 Report level label = 0.014 Pct Recovery = 87% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl SpecificMix = LB99392 Laboratory ID = 20133580036 Lab Value = 0.019 Expected Conc. = 0.0298 Report level label = 0.014 Pct Recovery = 65% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20131790009 Lab Value = 0.017 Expected Conc. = 0.0298 Report level label = 0.014 Pct Recovery = 56% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20131510026 Lab Value = 0.024 Expected Conc. = 0.0298 Report level label = 0.014 Pct Recovery = 81% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20180730064 Lab Value = 0.030 Expected Conc. = 0.0282 Report level label = 0.014 Pct Recovery = 105% Analysis Date = 05/16/18 SpikeMix = Abs 071717Pest: 30 µl & Abs 071817Pest: 30 µl SpecificMix = 071817Pest Laboratory ID = 20180050004 Lab Value = 0.027 Expected Conc. = 0.0282 Report level label = 0.014 Pct Recovery = 95% Analysis Date = 04/05/18 SpikeMix = Abs 071817Pest: 30 µl & ChemService 6472100: 30 µl SpecificMix = 071817Pest Laboratory ID = 20172780018 Lab Value = 0.028 Expected Conc. = 0.0282 Report level label = 0.014 Pct Recovery = 100% Analysis Date = 02/08/18 SpikeMix = ChemService 6537100: 30 µl & Abs 071817Pest: 30 µl SpecificMix = 071817Pest Laboratory ID = 20142470041 Lab Value = 0.022 Expected Conc. = 0.0279 Report level label = 0.014 Pct Recovery = 78% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141910243 Lab Value = 0.017 Expected Conc. = 0.0279 Report level label = 0.014 Pct Recovery = 62% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141640076 Lab Value = 0.019 Expected Conc. = 0.0279 Report level label = 0.014 Pct Recovery = 69% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141360094 Lab Value = 0.021 Expected Conc. = 0.0279 Report level label = 0.014 Pct Recovery = 74% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = E1140407002 Laboratory ID = 20150150115 Lab Value = 0.022 Expected Conc. = 0.0279 Report level label = 0.014 Pct Recovery = 79% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl SpecificMix = 032714 Laboratory ID = 20142820151 Lab Value = 0.022 Expected Conc. = 0.0279 Report level label = 0.014 Pct Recovery = 80% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl SpecificMix = 032714 Laboratory ID = 20141490205 Lab Value = 0.023 Expected Conc. = 0.0279 Report level label = 0.014 Pct Recovery = 81% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = 032714 Laboratory ID = 20141080004 Lab Value = 0.022 Expected Conc. = 0.0279 Report level label = 0.014 Pct Recovery = 77% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl SpecificMix = 032714 Laboratory ID = 20160430111 Lab Value = 0.017 Expected Conc. = 0.022 Report level label = 0.014 Pct Recovery = 79% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 3851600 Laboratory ID = 20160210080 Lab Value = 0.014 Expected Conc. = 0.022 Report level label = 0.014 Pct Recovery = 64% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 3851600 Laboratory ID = 20152950078 Lab Value = 0.011 Expected Conc. = 0.022 Report level label = 0.014 Pct Recovery = 51% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 3851600 Laboratory ID = 20153030068 Lab Value = 0.016 Expected Conc. = 0.022 Report level label = 0.014 Pct Recovery = 75% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = 3851600 Laboratory ID = 20151760208 Lab Value = 0.018 Expected Conc. = 0.022 Report level label = 0.014 Pct Recovery = 80% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl SpecificMix = 3851600 Laboratory ID = 20151380009 Lab Value = 0.014 Expected Conc. = 0.022 Report level label = 0.014 Pct Recovery = 64% Analysis Date = 05/30/15 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 3851600 Laboratory ID = 20152190003 Lab Value = 0.012 Expected Conc. = 0.021 Report level label = 0.014 Pct Recovery = 55% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = 0406-15-01 Laboratory ID = 20152040177 Lab Value = 0.022 Expected Conc. = 0.021 Report level label = 0.014 Pct Recovery = 106% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl SpecificMix = 0406-15-01 Laboratory ID = 20130510051 Lab Value = 0.019 Expected Conc. = 0.02 Report level label = 0.014 Pct Recovery = 97% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl SpecificMix = 0507-12-04.2 Laboratory ID = 20130390105 Lab Value = 0.013 Expected Conc. = 0.02 Report level label = 0.014 Pct Recovery = 65% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl SpecificMix = LB92783 Analysis Date = 06/19/18 Pct Recovery = 89% Analysis Date = 06/10/18 Pct Recovery = 88% Analysis Date = 06/10/18 Pct Recovery = 88% Analysis Date = 05/31/18 Pct Recovery = 88% Analysis Date = 05/31/18 Pct Recovery = 88% Analysis Date = 05/21/18 Pct Recovery = 88% Analysis Date = 05/21/18 Pct Recovery = 88% Analysis Date = 05/11/18 Pct Recovery = 88% Analysis Date = 05/11/18 Pct Recovery = 88% Analysis Date = 05/01/18 Pct Recovery = 87% Analysis Date = 05/01/18 Pct Recovery = 87% Analysis Date = 04/21/18 Pct Recovery = 87% Analysis Date = 04/21/18 Pct Recovery = 87% Analysis Date = 04/11/18 Pct Recovery = 87% Analysis Date = 04/11/18 Pct Recovery = 87% Analysis Date = 04/01/18 Pct Recovery = 86% Analysis Date = 04/01/18 Pct Recovery = 86% Analysis Date = 03/22/18 Pct Recovery = 86% Analysis Date = 03/22/18 Pct Recovery = 86% Analysis Date = 03/12/18 Pct Recovery = 86% Analysis Date = 03/12/18 Pct Recovery = 86% Analysis Date = 03/02/18 Pct Recovery = 86% Analysis Date = 03/02/18 Pct Recovery = 86% Analysis Date = 02/21/18 Pct Recovery = 85% Analysis Date = 02/21/18 Pct Recovery = 85% Analysis Date = 02/11/18 Pct Recovery = 85% Analysis Date = 02/11/18 Pct Recovery = 85% Analysis Date = 02/01/18 Pct Recovery = 85% Analysis Date = 02/01/18 Pct Recovery = 85% Analysis Date = 01/22/18 Pct Recovery = 84% Analysis Date = 01/22/18 Pct Recovery = 84% Analysis Date = 01/12/18 Pct Recovery = 84% Analysis Date = 01/12/18 Pct Recovery = 84% Analysis Date = 01/02/18 Pct Recovery = 84% Analysis Date = 01/02/18 Pct Recovery = 84% Analysis Date = 12/23/17 Pct Recovery = 84% Analysis Date = 12/23/17 Pct Recovery = 84% Analysis Date = 12/13/17 Pct Recovery = 83% Analysis Date = 12/13/17 Pct Recovery = 83% Analysis Date = 12/03/17 Pct Recovery = 83% Analysis Date = 12/03/17 Pct Recovery = 83% Analysis Date = 11/23/17 Pct Recovery = 83% Analysis Date = 11/23/17 Pct Recovery = 83% Analysis Date = 11/13/17 Pct Recovery = 82% Analysis Date = 11/13/17 Pct Recovery = 82% Analysis Date = 11/04/17 Pct Recovery = 82% Analysis Date = 11/04/17 Pct Recovery = 82% Analysis Date = 10/25/17 Pct Recovery = 82% Analysis Date = 10/25/17 Pct Recovery = 82% Analysis Date = 10/15/17 Pct Recovery = 82% Analysis Date = 10/15/17 Pct Recovery = 82% Analysis Date = 10/05/17 Pct Recovery = 81% Analysis Date = 10/05/17 Pct Recovery = 81% Analysis Date = 09/25/17 Pct Recovery = 81% Analysis Date = 09/25/17 Pct Recovery = 81% Analysis Date = 09/15/17 Pct Recovery = 81% Analysis Date = 09/15/17 Pct Recovery = 81% Analysis Date = 09/05/17 Pct Recovery = 81% Analysis Date = 09/05/17 Pct Recovery = 81% Analysis Date = 08/26/17 Pct Recovery = 80% Analysis Date = 08/26/17 Pct Recovery = 80% Analysis Date = 08/16/17 Pct Recovery = 80% Analysis Date = 08/16/17 Pct Recovery = 80% Analysis Date = 08/06/17 Pct Recovery = 80% Analysis Date = 08/06/17 Pct Recovery = 80% Analysis Date = 07/27/17 Pct Recovery = 79% Analysis Date = 07/27/17 Pct Recovery = 79% Analysis Date = 07/18/17 Pct Recovery = 79% Analysis Date = 07/18/17 Pct Recovery = 79% Analysis Date = 07/08/17 Pct Recovery = 79% Analysis Date = 07/08/17 Pct Recovery = 79% Analysis Date = 06/28/17 Pct Recovery = 79% Analysis Date = 06/28/17 Pct Recovery = 79% Analysis Date = 06/18/17 Pct Recovery = 78% Analysis Date = 06/18/17 Pct Recovery = 78% Analysis Date = 06/08/17 Pct Recovery = 78% Analysis Date = 06/08/17 Pct Recovery = 78% Analysis Date = 05/29/17 Pct Recovery = 78% Analysis Date = 05/29/17 Pct Recovery = 78% Analysis Date = 05/19/17 Pct Recovery = 77% Analysis Date = 05/19/17 Pct Recovery = 77% Analysis Date = 05/09/17 Pct Recovery = 77% Analysis Date = 05/09/17 Pct Recovery = 77% Analysis Date = 04/29/17 Pct Recovery = 77% Analysis Date = 04/29/17 Pct Recovery = 77% Analysis Date = 04/19/17 Pct Recovery = 77% Analysis Date = 04/19/17 Pct Recovery = 77% Analysis Date = 04/09/17 Pct Recovery = 76% Analysis Date = 04/09/17 Pct Recovery = 76% Analysis Date = 03/31/17 Pct Recovery = 76% Analysis Date = 03/31/17 Pct Recovery = 76% Analysis Date = 03/21/17 Pct Recovery = 76% Analysis Date = 03/21/17 Pct Recovery = 76% Analysis Date = 03/11/17 Pct Recovery = 75% Analysis Date = 03/11/17 Pct Recovery = 75% Analysis Date = 03/01/17 Pct Recovery = 75% Analysis Date = 03/01/17 Pct Recovery = 75% Analysis Date = 02/19/17 Pct Recovery = 75% Analysis Date = 02/19/17 Pct Recovery = 75% Analysis Date = 02/09/17 Pct Recovery = 75% Analysis Date = 02/09/17 Pct Recovery = 75% Analysis Date = 01/30/17 Pct Recovery = 75% Analysis Date = 01/30/17 Pct Recovery = 75% Analysis Date = 01/20/17 Pct Recovery = 74% Analysis Date = 01/20/17 Pct Recovery = 74% Analysis Date = 01/10/17 Pct Recovery = 74% Analysis Date = 01/10/17 Pct Recovery = 74% Analysis Date = 12/31/16 Pct Recovery = 74% Analysis Date = 12/31/16 Pct Recovery = 74% Analysis Date = 12/21/16 Pct Recovery = 74% Analysis Date = 12/21/16 Pct Recovery = 74% Analysis Date = 12/12/16 Pct Recovery = 73% Analysis Date = 12/12/16 Pct Recovery = 73% Analysis Date = 12/02/16 Pct Recovery = 73% Analysis Date = 12/02/16 Pct Recovery = 73% Analysis Date = 11/22/16 Pct Recovery = 73% Analysis Date = 11/22/16 Pct Recovery = 73% Analysis Date = 11/12/16 Pct Recovery = 73% Analysis Date = 11/12/16 Pct Recovery = 73% Analysis Date = 11/02/16 Pct Recovery = 72% Analysis Date = 11/02/16 Pct Recovery = 72% Analysis Date = 10/23/16 Pct Recovery = 72% Analysis Date = 10/23/16 Pct Recovery = 72% Analysis Date = 10/13/16 Pct Recovery = 72% Analysis Date = 10/13/16 Pct Recovery = 72% Analysis Date = 10/03/16 Pct Recovery = 72% Analysis Date = 10/03/16 Pct Recovery = 72% Analysis Date = 09/23/16 Pct Recovery = 72% Analysis Date = 09/23/16 Pct Recovery = 72% Analysis Date = 09/13/16 Pct Recovery = 71% Analysis Date = 09/13/16 Pct Recovery = 71% Analysis Date = 09/03/16 Pct Recovery = 71% Analysis Date = 09/03/16 Pct Recovery = 71% Analysis Date = 08/25/16 Pct Recovery = 71% Analysis Date = 08/25/16 Pct Recovery = 71% Analysis Date = 08/15/16 Pct Recovery = 71% Analysis Date = 08/15/16 Pct Recovery = 71% Analysis Date = 08/05/16 Pct Recovery = 71% Analysis Date = 08/05/16 Pct Recovery = 71% Analysis Date = 07/26/16 Pct Recovery = 71% Analysis Date = 07/26/16 Pct Recovery = 71% Analysis Date = 07/16/16 Pct Recovery = 71% Analysis Date = 07/16/16 Pct Recovery = 71% Analysis Date = 07/06/16 Pct Recovery = 71% Analysis Date = 07/06/16 Pct Recovery = 71% Analysis Date = 06/26/16 Pct Recovery = 70% Analysis Date = 06/26/16 Pct Recovery = 70% Analysis Date = 06/16/16 Pct Recovery = 70% Analysis Date = 06/16/16 Pct Recovery = 70% Analysis Date = 06/06/16 Pct Recovery = 70% Analysis Date = 06/06/16 Pct Recovery = 70% Analysis Date = 05/27/16 Pct Recovery = 70% Analysis Date = 05/27/16 Pct Recovery = 70% Analysis Date = 05/17/16 Pct Recovery = 70% Analysis Date = 05/17/16 Pct Recovery = 70% Analysis Date = 05/08/16 Pct Recovery = 70% Analysis Date = 05/08/16 Pct Recovery = 70% Analysis Date = 04/28/16 Pct Recovery = 70% Analysis Date = 04/28/16 Pct Recovery = 70% Analysis Date = 04/18/16 Pct Recovery = 70% Analysis Date = 04/18/16 Pct Recovery = 70% Analysis Date = 04/08/16 Pct Recovery = 70% Analysis Date = 04/08/16 Pct Recovery = 70% Analysis Date = 03/29/16 Pct Recovery = 70% Analysis Date = 03/29/16 Pct Recovery = 70% Analysis Date = 03/19/16 Pct Recovery = 70% Analysis Date = 03/19/16 Pct Recovery = 70% Analysis Date = 03/09/16 Pct Recovery = 69% Analysis Date = 03/09/16 Pct Recovery = 69% Analysis Date = 02/28/16 Pct Recovery = 69% Analysis Date = 02/28/16 Pct Recovery = 69% Analysis Date = 02/18/16 Pct Recovery = 69% Analysis Date = 02/18/16 Pct Recovery = 69% Analysis Date = 02/08/16 Pct Recovery = 69% Analysis Date = 02/08/16 Pct Recovery = 69% Analysis Date = 01/29/16 Pct Recovery = 69% Analysis Date = 01/29/16 Pct Recovery = 69% Analysis Date = 01/20/16 Pct Recovery = 69% Analysis Date = 01/20/16 Pct Recovery = 69% Analysis Date = 01/10/16 Pct Recovery = 69% Analysis Date = 01/10/16 Pct Recovery = 69% Analysis Date = 12/31/15 Pct Recovery = 69% Analysis Date = 12/31/15 Pct Recovery = 69% Analysis Date = 12/21/15 Pct Recovery = 69% Analysis Date = 12/21/15 Pct Recovery = 69% Analysis Date = 12/11/15 Pct Recovery = 69% Analysis Date = 12/11/15 Pct Recovery = 69% Analysis Date = 12/01/15 Pct Recovery = 69% Analysis Date = 12/01/15 Pct Recovery = 69% Analysis Date = 11/21/15 Pct Recovery = 69% Analysis Date = 11/21/15 Pct Recovery = 69% Analysis Date = 11/11/15 Pct Recovery = 69% Analysis Date = 11/11/15 Pct Recovery = 69% Analysis Date = 11/01/15 Pct Recovery = 69% Analysis Date = 11/01/15 Pct Recovery = 69% Analysis Date = 10/22/15 Pct Recovery = 69% Analysis Date = 10/22/15 Pct Recovery = 69% Analysis Date = 10/12/15 Pct Recovery = 69% Analysis Date = 10/12/15 Pct Recovery = 69% Analysis Date = 10/02/15 Pct Recovery = 69% Analysis Date = 10/02/15 Pct Recovery = 69% Analysis Date = 09/23/15 Pct Recovery = 69% Analysis Date = 09/23/15 Pct Recovery = 69% Analysis Date = 09/13/15 Pct Recovery = 69% Analysis Date = 09/13/15 Pct Recovery = 69% Analysis Date = 09/03/15 Pct Recovery = 69% Analysis Date = 09/03/15 Pct Recovery = 69% Analysis Date = 08/24/15 Pct Recovery = 69% Analysis Date = 08/24/15 Pct Recovery = 69% Analysis Date = 08/14/15 Pct Recovery = 69% Analysis Date = 08/14/15 Pct Recovery = 69% Analysis Date = 08/04/15 Pct Recovery = 69% Analysis Date = 08/04/15 Pct Recovery = 69% Analysis Date = 07/25/15 Pct Recovery = 69% Analysis Date = 07/25/15 Pct Recovery = 69% Analysis Date = 07/15/15 Pct Recovery = 69% Analysis Date = 07/15/15 Pct Recovery = 69% Analysis Date = 07/05/15 Pct Recovery = 70% Analysis Date = 07/05/15 Pct Recovery = 70% Analysis Date = 06/25/15 Pct Recovery = 70% Analysis Date = 06/25/15 Pct Recovery = 70% Analysis Date = 06/15/15 Pct Recovery = 70% Analysis Date = 06/15/15 Pct Recovery = 70% Analysis Date = 06/06/15 Pct Recovery = 70% Analysis Date = 06/06/15 Pct Recovery = 70% Analysis Date = 05/27/15 Pct Recovery = 70% Analysis Date = 05/27/15 Pct Recovery = 70% Analysis Date = 05/17/15 Pct Recovery = 70% Analysis Date = 05/17/15 Pct Recovery = 70% Analysis Date = 05/07/15 Pct Recovery = 70% Analysis Date = 05/07/15 Pct Recovery = 70% Analysis Date = 04/27/15 Pct Recovery = 70% Analysis Date = 04/27/15 Pct Recovery = 70% Analysis Date = 04/17/15 Pct Recovery = 70% Analysis Date = 04/17/15 Pct Recovery = 70% Analysis Date = 04/07/15 Pct Recovery = 70% Analysis Date = 04/07/15 Pct Recovery = 70% Analysis Date = 03/28/15 Pct Recovery = 70% Analysis Date = 03/28/15 Pct Recovery = 70% Analysis Date = 03/18/15 Pct Recovery = 71% Analysis Date = 03/18/15 Pct Recovery = 71% Analysis Date = 03/08/15 Pct Recovery = 71% Analysis Date = 03/08/15 Pct Recovery = 71% Analysis Date = 02/26/15 Pct Recovery = 71% Analysis Date = 02/26/15 Pct Recovery = 71% Analysis Date = 02/17/15 Pct Recovery = 71% Analysis Date = 02/17/15 Pct Recovery = 71% Analysis Date = 02/07/15 Pct Recovery = 71% Analysis Date = 02/07/15 Pct Recovery = 71% Analysis Date = 01/28/15 Pct Recovery = 71% Analysis Date = 01/28/15 Pct Recovery = 71% Analysis Date = 01/18/15 Pct Recovery = 71% Analysis Date = 01/18/15 Pct Recovery = 71% Analysis Date = 01/08/15 Pct Recovery = 71% Analysis Date = 01/08/15 Pct Recovery = 71% Analysis Date = 12/29/14 Pct Recovery = 71% Analysis Date = 12/29/14 Pct Recovery = 71% Analysis Date = 12/19/14 Pct Recovery = 72% Analysis Date = 12/19/14 Pct Recovery = 72% Analysis Date = 12/09/14 Pct Recovery = 72% Analysis Date = 12/09/14 Pct Recovery = 72% Analysis Date = 11/29/14 Pct Recovery = 72% Analysis Date = 11/29/14 Pct Recovery = 72% Analysis Date = 11/19/14 Pct Recovery = 72% Analysis Date = 11/19/14 Pct Recovery = 72% Analysis Date = 11/09/14 Pct Recovery = 72% Analysis Date = 11/09/14 Pct Recovery = 72% Analysis Date = 10/31/14 Pct Recovery = 72% Analysis Date = 10/31/14 Pct Recovery = 72% Analysis Date = 10/21/14 Pct Recovery = 72% Analysis Date = 10/21/14 Pct Recovery = 72% Analysis Date = 10/11/14 Pct Recovery = 72% Analysis Date = 10/11/14 Pct Recovery = 72% Analysis Date = 10/01/14 Pct Recovery = 72% Analysis Date = 10/01/14 Pct Recovery = 72% Analysis Date = 09/21/14 Pct Recovery = 73% Analysis Date = 09/21/14 Pct Recovery = 73% Analysis Date = 09/11/14 Pct Recovery = 73% Analysis Date = 09/11/14 Pct Recovery = 73% Analysis Date = 09/01/14 Pct Recovery = 73% Analysis Date = 09/01/14 Pct Recovery = 73% Analysis Date = 08/22/14 Pct Recovery = 73% Analysis Date = 08/22/14 Pct Recovery = 73% Analysis Date = 08/12/14 Pct Recovery = 73% Analysis Date = 08/12/14 Pct Recovery = 73% Analysis Date = 08/02/14 Pct Recovery = 73% Analysis Date = 08/02/14 Pct Recovery = 73% Analysis Date = 07/23/14 Pct Recovery = 73% Analysis Date = 07/23/14 Pct Recovery = 73% Analysis Date = 07/14/14 Pct Recovery = 73% Analysis Date = 07/14/14 Pct Recovery = 73% Analysis Date = 07/04/14 Pct Recovery = 73% Analysis Date = 07/04/14 Pct Recovery = 73% Analysis Date = 06/24/14 Pct Recovery = 73% Analysis Date = 06/24/14 Pct Recovery = 73% Analysis Date = 06/14/14 Pct Recovery = 73% Analysis Date = 06/14/14 Pct Recovery = 73% Analysis Date = 06/04/14 Pct Recovery = 73% Analysis Date = 06/04/14 Pct Recovery = 73% Analysis Date = 05/25/14 Pct Recovery = 73% Analysis Date = 05/25/14 Pct Recovery = 73% Analysis Date = 05/15/14 Pct Recovery = 74% Analysis Date = 05/15/14 Pct Recovery = 74% Analysis Date = 05/05/14 Pct Recovery = 74% Analysis Date = 05/05/14 Pct Recovery = 74% Analysis Date = 04/25/14 Pct Recovery = 74% Analysis Date = 04/25/14 Pct Recovery = 74% Analysis Date = 04/15/14 Pct Recovery = 74% Analysis Date = 04/15/14 Pct Recovery = 74% Analysis Date = 04/05/14 Pct Recovery = 74% Analysis Date = 04/05/14 Pct Recovery = 74% Analysis Date = 03/27/14 Pct Recovery = 74% Analysis Date = 03/27/14 Pct Recovery = 74% Analysis Date = 03/17/14 Pct Recovery = 74% Analysis Date = 03/17/14 Pct Recovery = 74% Analysis Date = 03/07/14 Pct Recovery = 74% Analysis Date = 03/07/14 Pct Recovery = 74% Analysis Date = 02/25/14 Pct Recovery = 74% Analysis Date = 02/25/14 Pct Recovery = 74% Analysis Date = 02/15/14 Pct Recovery = 74% Analysis Date = 02/15/14 Pct Recovery = 74% Analysis Date = 02/05/14 Pct Recovery = 74% Analysis Date = 02/05/14 Pct Recovery = 74% Analysis Date = 01/26/14 Pct Recovery = 74% Analysis Date = 01/26/14 Pct Recovery = 74% Analysis Date = 01/16/14 Pct Recovery = 74% Analysis Date = 01/16/14 Pct Recovery = 74% Analysis Date = 01/06/14 Pct Recovery = 74% Analysis Date = 01/06/14 Pct Recovery = 74% Analysis Date = 12/27/13 Pct Recovery = 74% Analysis Date = 12/27/13 Pct Recovery = 74% Analysis Date = 12/17/13 Pct Recovery = 74% Analysis Date = 12/17/13 Pct Recovery = 74% Analysis Date = 12/08/13 Pct Recovery = 74% Analysis Date = 12/08/13 Pct Recovery = 74% Analysis Date = 11/28/13 Pct Recovery = 75% Analysis Date = 11/28/13 Pct Recovery = 75% Analysis Date = 11/18/13 Pct Recovery = 75% Analysis Date = 11/18/13 Pct Recovery = 75% Analysis Date = 11/08/13 Pct Recovery = 75% Analysis Date = 11/08/13 Pct Recovery = 75% Analysis Date = 10/29/13 Pct Recovery = 75% Analysis Date = 10/29/13 Pct Recovery = 75% Analysis Date = 10/19/13 Pct Recovery = 75% Analysis Date = 10/19/13 Pct Recovery = 75% Analysis Date = 10/09/13 Pct Recovery = 75% Analysis Date = 10/09/13 Pct Recovery = 75% Analysis Date = 09/29/13 Pct Recovery = 75% Analysis Date = 09/29/13 Pct Recovery = 75% Analysis Date = 09/19/13 Pct Recovery = 75% Analysis Date = 09/19/13 Pct Recovery = 75% Analysis Date = 09/09/13 Pct Recovery = 75% Analysis Date = 09/09/13 Pct Recovery = 75% Analysis Date = 08/30/13 Pct Recovery = 75% Analysis Date = 08/30/13 Pct Recovery = 75% Analysis Date = 08/21/13 Pct Recovery = 75% Analysis Date = 08/21/13 Pct Recovery = 75% Analysis Date = 08/11/13 Pct Recovery = 75% Analysis Date = 08/11/13 Pct Recovery = 75% Analysis Date = 08/01/13 Pct Recovery = 75% Analysis Date = 08/01/13 Pct Recovery = 75% Analysis Date = 07/22/13 Pct Recovery = 75% Analysis Date = 07/22/13 Pct Recovery = 75% Analysis Date = 07/12/13 Pct Recovery = 76% Analysis Date = 07/12/13 Pct Recovery = 76% Analysis Date = 07/02/13 Pct Recovery = 76% Analysis Date = 07/02/13 Pct Recovery = 76% Analysis Date = 06/22/13 Pct Recovery = 76% Analysis Date = 06/22/13 Pct Recovery = 76% Analysis Date = 06/12/13 Pct Recovery = 76% Analysis Date = 06/12/13 Pct Recovery = 76% Analysis Date = 06/02/13 Pct Recovery = 76% Analysis Date = 06/02/13 Pct Recovery = 76% Analysis Date = 05/23/13 Pct Recovery = 76% Analysis Date = 05/23/13 Pct Recovery = 76% Analysis Date = 05/13/13 Pct Recovery = 76% Analysis Date = 05/13/13 Pct Recovery = 76% Analysis Date = 05/04/13 Pct Recovery = 76% Analysis Date = 05/04/13 Pct Recovery = 76% Analysis Date = 04/24/13 Pct Recovery = 76% Analysis Date = 04/24/13 Pct Recovery = 76% Analysis Date = 04/14/13 Pct Recovery = 76% Analysis Date = 04/14/13 Pct Recovery = 76% Analysis Date = 04/04/13 Pct Recovery = 76% Analysis Date = 04/04/13 Pct Recovery = 76% Analysis Date = 03/25/13 Pct Recovery = 76% Analysis Date = 03/25/13 Pct Recovery = 76% Analysis Date = 03/15/13 Pct Recovery = 76% Analysis Date = 03/15/13 Pct Recovery = 76% Analysis Date = 03/05/13 Pct Recovery = 76% Analysis Date = 03/05/13 Pct Recovery = 76% Analysis Date = 02/23/13 Pct Recovery = 76% Analysis Date = 02/23/13 Pct Recovery = 76% Analysis Date = 02/13/13 Pct Recovery = 77% Analysis Date = 02/13/13 Pct Recovery = 77% Analysis Date = 02/03/13 Pct Recovery = 77% Analysis Date = 02/03/13 Pct Recovery = 77% Analysis Date = 01/24/13 Pct Recovery = 77% Analysis Date = 01/24/13 Pct Recovery = 77% Analysis Date = 01/15/13 Pct Recovery = 77% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
BENFLURALIN

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 72 74% 14% 72% 12%
Total 72 74% 14% 72% 12%

Sample Statistics
BENFLURALIN

Characteristic N % % Basis
Plotted 72 99% Spiked
Estimated Values 1 1% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 73 .  
False Negatives 1 1% 1 out of 73
Not Spiked 61 .  
False Positives 1 2% 1 out of 61

OBSP Determination:
CARBARYL
METHOD: 2033 , TESTIDCODE: 82680GCM35

Laboratory ID = 20140100085 Lab Value = 0.712 Expected Conc. = 0.701 Report level label = 0.06 Pct Recovery = 102% Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl SpecificMix = 042413 Laboratory ID = 20180390003 Lab Value = 0.188 Expected Conc. = 0.402 Report level label = 0.06 Pct Recovery = 47% Analysis Date = 04/06/18 SpikeMix = Spex Organics EN170808006: 100 µl & Abs 071717Pest: 100 µl SpecificMix = EN170808006 Laboratory ID = 20163370001 Lab Value = 0.265 Expected Conc. = 0.373 Report level label = 0.06 Pct Recovery = 71% Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl SpecificMix = B20160331 Laboratory ID = 20163150006 Lab Value = 0.264 Expected Conc. = 0.373 Report level label = 0.06 Pct Recovery = 71% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl SpecificMix = B20160331 Laboratory ID = 20161880109 Lab Value = 0.352 Expected Conc. = 0.373 Report level label = 0.06 Pct Recovery = 94% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl SpecificMix = 03FF076 Laboratory ID = 20130250061 Lab Value = 0.282 Expected Conc. = 0.373 Report level label = 0.06 Pct Recovery = 76% Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl SpecificMix = 05BB029 Laboratory ID = 20152750006 Lab Value = 0.191 Expected Conc. = 0.36 Report level label = 0.06 Pct Recovery = 53% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl SpecificMix = EN150514012 Laboratory ID = 20152460215 Lab Value = 0.262 Expected Conc. = 0.36 Report level label = 0.06 Pct Recovery = 73% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl SpecificMix = EN150514012 Laboratory ID = 20132690010 Lab Value = 0.330 Expected Conc. = 0.3505 Report level label = 0.06 Pct Recovery = 94% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl SpecificMix = 042413 Laboratory ID = 20132560001 Lab Value = 0.259 Expected Conc. = 0.3505 Report level label = 0.06 Pct Recovery = 74% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl SpecificMix = 042413 Laboratory ID = 20132140002 Lab Value = 0.282 Expected Conc. = 0.3485 Report level label = 0.06 Pct Recovery = 81% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl SpecificMix = 04CC101 Laboratory ID = 20171720140 Lab Value = 0.268 Expected Conc. = 0.2984 Report level label = 0.06 Pct Recovery = 90% Analysis Date = 08/31/17 SpikeMix = Supelco LC20138V: 80 µl & Phenova B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20171660002 Lab Value = 0.295 Expected Conc. = 0.2984 Report level label = 0.06 Pct Recovery = 99% Analysis Date = 08/23/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20170960001 Lab Value = 0.250 Expected Conc. = 0.2984 Report level label = 0.06 Pct Recovery = 84% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl SpecificMix = 03FF076 Laboratory ID = 20170190026 Lab Value = 0.223 Expected Conc. = 0.2984 Report level label = 0.06 Pct Recovery = 75% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20161470001 Lab Value = 0.240 Expected Conc. = 0.2984 Report level label = 0.06 Pct Recovery = 80% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20150720069 Lab Value = 0.142 Expected Conc. = 0.243 Report level label = 0.06 Pct Recovery = 58% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 0227-14-08 Laboratory ID = 20141770149 Lab Value = 0.143 Expected Conc. = 0.243 Report level label = 0.06 Pct Recovery = 59% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl SpecificMix = 0227-14-08 Laboratory ID = 20141570088 Lab Value = 0.209 Expected Conc. = 0.243 Report level label = 0.06 Pct Recovery = 86% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl SpecificMix = 0227-14-08 Laboratory ID = 20150430092 Lab Value = 0.127 Expected Conc. = 0.24 Report level label = 0.06 Pct Recovery = 53% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl SpecificMix = 042814 Laboratory ID = 20143240095 Lab Value = 0.228 Expected Conc. = 0.24 Report level label = 0.06 Pct Recovery = 95% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl SpecificMix = 042814 Laboratory ID = 20142960086 Lab Value = 0.144 Expected Conc. = 0.24 Report level label = 0.06 Pct Recovery = 60% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 042814 Laboratory ID = 20142530087 Lab Value = 0.148 Expected Conc. = 0.24 Report level label = 0.06 Pct Recovery = 62% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl SpecificMix = 042814 Laboratory ID = 20181430122 Lab Value = 0.120 Expected Conc. = 0.201 Report level label = 0.06 Pct Recovery = 60% Analysis Date = 06/20/18 SpikeMix = Abs 071817Pest: 50 µl & Spex Organics EN170808006: 50 µl SpecificMix = EN170808006 Laboratory ID = 20172560101 Lab Value = 0.104 Expected Conc. = 0.201 Report level label = 0.06 Pct Recovery = 52% Analysis Date = 12/22/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6567600: 50 µl SpecificMix = EN170808006 Laboratory ID = 20172370001 Lab Value = 0.120 Expected Conc. = 0.201 Report level label = 0.06 Pct Recovery = 60% Analysis Date = 11/18/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6537100: 50 µl SpecificMix = EN170808006 Laboratory ID = 20172230001 Lab Value = 0.165 Expected Conc. = 0.2 Report level label = 0.06 Pct Recovery = 83% Analysis Date = 10/19/17 SpikeMix = ChemService 6472100: 50 µl & Abs 071717Pest: 50 µl SpecificMix = 6472100 Laboratory ID = 20130940097 Lab Value = 0.127 Expected Conc. = 0.189 Report level label = 0.06 Pct Recovery = 67% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = 052412 Laboratory ID = 20130100066 Lab Value = 0.176 Expected Conc. = 0.189 Report level label = 0.06 Pct Recovery = 93% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl SpecificMix = 052412 Laboratory ID = 20140230082 Lab Value = 0.136 Expected Conc. = 0.188 Report level label = 0.06 Pct Recovery = 72% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl SpecificMix = 012513 Laboratory ID = 20132420001 Lab Value = 0.155 Expected Conc. = 0.188 Report level label = 0.06 Pct Recovery = 82% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl SpecificMix = 012513 Laboratory ID = 20160630046 Lab Value = 0.090 Expected Conc. = 0.18 Report level label = 0.06 Pct Recovery = 50% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = EN150514012 Laboratory ID = 20153440001 Lab Value = 0.102 Expected Conc. = 0.18 Report level label = 0.06 Pct Recovery = 57% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = EN150514012 Laboratory ID = 20152330039 Lab Value = 0.119 Expected Conc. = 0.18 Report level label = 0.06 Pct Recovery = 66% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl SpecificMix = 041415 Laboratory ID = 20151900132 Lab Value = 0.140 Expected Conc. = 0.18 Report level label = 0.06 Pct Recovery = 78% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl SpecificMix = 041415 Laboratory ID = 20151270112 Lab Value = 0.124 Expected Conc. = 0.18 Report level label = 0.06 Pct Recovery = 69% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl SpecificMix = 041415 Laboratory ID = 20172020035 Lab Value = 0.127 Expected Conc. = 0.1492 Report level label = 0.06 Pct Recovery = 85% Analysis Date = 11/07/17 SpikeMix = Abs 071717Pest: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20171510080 Lab Value = 0.127 Expected Conc. = 0.1492 Report level label = 0.06 Pct Recovery = 85% Analysis Date = 06/09/17 SpikeMix = Supelco LC20138V: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20171160110 Lab Value = 0.100 Expected Conc. = 0.1492 Report level label = 0.06 Pct Recovery = 67% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = B20160331 Laboratory ID = 20170460061 Lab Value = 0.118 Expected Conc. = 0.1492 Report level label = 0.06 Pct Recovery = 79% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl SpecificMix = 03FF076 Laboratory ID = 20162660005 Lab Value = 0.089 Expected Conc. = 0.1492 Report level label = 0.06 Pct Recovery = 60% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl SpecificMix = 03FF076 Laboratory ID = 20162380004 Lab Value = 0.123 Expected Conc. = 0.1492 Report level label = 0.06 Pct Recovery = 82% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = B20160331 Laboratory ID = 20162150213 Lab Value = 0.079 Expected Conc. = 0.1492 Report level label = 0.06 Pct Recovery = 53% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl SpecificMix = B20160331 Laboratory ID = 20161600087 Lab Value = 0.102 Expected Conc. = 0.1492 Report level label = 0.06 Pct Recovery = 68% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20161340228 Lab Value = 0.095 Expected Conc. = 0.1492 Report level label = 0.06 Pct Recovery = 64% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl SpecificMix = 03FF076 Laboratory ID = 20161190075 Lab Value = 0.081 Expected Conc. = 0.1492 Report level label = 0.06 Pct Recovery = 54% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20133580036 Lab Value = 0.119 Expected Conc. = 0.1402 Report level label = 0.06 Pct Recovery = 85% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 042413 Laboratory ID = 20133190012 Lab Value = 0.128 Expected Conc. = 0.1402 Report level label = 0.06 Pct Recovery = 91% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 042413 Laboratory ID = 20131650073 Lab Value = 0.148 Expected Conc. = 0.1402 Report level label = 0.06 Pct Recovery = 106% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl SpecificMix = 042413 Laboratory ID = 20140730138 Lab Value = 0.091 Expected Conc. = 0.1394 Report level label = 0.06 Pct Recovery = 65% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 04CC101 Laboratory ID = 20140510043 Lab Value = 0.076 Expected Conc. = 0.1394 Report level label = 0.06 Pct Recovery = 55% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 04CC101 Laboratory ID = 20133310030 Lab Value = 0.113 Expected Conc. = 0.1394 Report level label = 0.06 Pct Recovery = 81% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl SpecificMix = 04CC101 Laboratory ID = 20132280016 Lab Value = 0.126 Expected Conc. = 0.1394 Report level label = 0.06 Pct Recovery = 90% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl SpecificMix = 04CC101 Laboratory ID = 20131510026 Lab Value = 0.100 Expected Conc. = 0.1394 Report level label = 0.06 Pct Recovery = 72% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl SpecificMix = 04CC101 Laboratory ID = 20141840097 Lab Value = 0.083 Expected Conc. = 0.1215 Report level label = 0.06 Pct Recovery = 68% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20141490205 Lab Value = 0.108 Expected Conc. = 0.1215 Report level label = 0.06 Pct Recovery = 89% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20141420140 Lab Value = 0.085 Expected Conc. = 0.1215 Report level label = 0.06 Pct Recovery = 70% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20141360094 Lab Value = 0.091 Expected Conc. = 0.1215 Report level label = 0.06 Pct Recovery = 75% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20180940080 Lab Value = 0.068 Expected Conc. = 0.12 Report level label = 0.06 Pct Recovery = 57% Analysis Date = 05/31/18 SpikeMix = ChemService 6472100: 30 µl & Abs 071717Pest: 30 µl SpecificMix = 6472100 Laboratory ID = 20180050004 Lab Value = 0.089 Expected Conc. = 0.12 Report level label = 0.06 Pct Recovery = 74% Analysis Date = 04/05/18 SpikeMix = Abs 071817Pest: 30 µl & ChemService 6472100: 30 µl SpecificMix = 6472100 Laboratory ID = 20173120093 Lab Value = 0.088 Expected Conc. = 0.12 Report level label = 0.06 Pct Recovery = 73% Analysis Date = 03/10/18 SpikeMix = ChemService 6472100: 30 µl & ChemService 6537100: 30 µl SpecificMix = 6472100 Laboratory ID = 20143370094 Lab Value = 0.069 Expected Conc. = 0.12 Report level label = 0.06 Pct Recovery = 58% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl SpecificMix = 042814 Laboratory ID = 20142820151 Lab Value = 0.094 Expected Conc. = 0.12 Report level label = 0.06 Pct Recovery = 78% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl SpecificMix = 042814 Laboratory ID = 20142470041 Lab Value = 0.114 Expected Conc. = 0.12 Report level label = 0.06 Pct Recovery = 95% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl SpecificMix = 042814 Laboratory ID = 20142200164 Lab Value = 0.083 Expected Conc. = 0.12 Report level label = 0.06 Pct Recovery = 69% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 042814 Laboratory ID = 20161050143 Lab Value = 0.058 Expected Conc. = 0.09 Report level label = 0.06 Pct Recovery = 64% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 041415 Laboratory ID = 20160560044 Lab Value = 0.048 Expected Conc. = 0.09 Report level label = 0.06 Pct Recovery = 53% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl SpecificMix = 041415 Laboratory ID = 20160210080 Lab Value = 0.040 Expected Conc. = 0.09 Report level label = 0.06 Pct Recovery = 44% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 041415 Laboratory ID = 20160070059 Lab Value = 0.067 Expected Conc. = 0.09 Report level label = 0.06 Pct Recovery = 74% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = EN150514012 Laboratory ID = 20153160001 Lab Value = 0.045 Expected Conc. = 0.09 Report level label = 0.06 Pct Recovery = 50% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = EN150514012 Laboratory ID = 20152950078 Lab Value = 0.039 Expected Conc. = 0.09 Report level label = 0.06 Pct Recovery = 43% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 041415 Laboratory ID = 20152040177 Lab Value = 0.075 Expected Conc. = 0.09 Report level label = 0.06 Pct Recovery = 83% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl SpecificMix = 041415 Laboratory ID = 20151760208 Lab Value = 0.073 Expected Conc. = 0.09 Report level label = 0.06 Pct Recovery = 81% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl SpecificMix = EN150514012 Laboratory ID = 20151480170 Lab Value = 0.061 Expected Conc. = 0.09 Report level label = 0.06 Pct Recovery = 68% Analysis Date = 06/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150514012 Laboratory ID = 20151210037 Lab Value = 0.074 Expected Conc. = 0.09 Report level label = 0.06 Pct Recovery = 82% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 041415 Laboratory ID = 20133400002 Lab Value = 0.085 Expected Conc. = 0.0756 Report level label = 0.06 Pct Recovery = 112% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = 052412 Laboratory ID = 20132910008 Lab Value = 0.060 Expected Conc. = 0.0756 Report level label = 0.06 Pct Recovery = 79% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = 052412 Laboratory ID = 20130650005 Lab Value = 0.053 Expected Conc. = 0.0756 Report level label = 0.06 Pct Recovery = 70% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl SpecificMix = 052412 Laboratory ID = 20140860102 Lab Value = 0.060 Expected Conc. = 0.0752 Report level label = 0.06 Pct Recovery = 80% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 012513 Laboratory ID = 20131920149 Lab Value = 0.065 Expected Conc. = 0.0752 Report level label = 0.06 Pct Recovery = 86% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl SpecificMix = 012513 Laboratory ID = 20131230084 Lab Value = 0.086 Expected Conc. = 0.0746 Report level label = 0.06 Pct Recovery = 115% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl SpecificMix = 05BB029 Laboratory ID = 20130510051 Lab Value = 0.064 Expected Conc. = 0.0746 Report level label = 0.06 Pct Recovery = 86% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl SpecificMix = 05BB029 Analysis Date = 06/20/18 Pct Recovery = 72% Analysis Date = 06/10/18 Pct Recovery = 72% Analysis Date = 06/10/18 Pct Recovery = 72% Analysis Date = 05/31/18 Pct Recovery = 72% Analysis Date = 05/31/18 Pct Recovery = 72% Analysis Date = 05/21/18 Pct Recovery = 72% Analysis Date = 05/21/18 Pct Recovery = 72% Analysis Date = 05/11/18 Pct Recovery = 72% Analysis Date = 05/11/18 Pct Recovery = 72% Analysis Date = 05/01/18 Pct Recovery = 72% Analysis Date = 05/01/18 Pct Recovery = 72% Analysis Date = 04/21/18 Pct Recovery = 72% Analysis Date = 04/21/18 Pct Recovery = 72% Analysis Date = 04/11/18 Pct Recovery = 72% Analysis Date = 04/11/18 Pct Recovery = 72% Analysis Date = 04/01/18 Pct Recovery = 72% Analysis Date = 04/01/18 Pct Recovery = 72% Analysis Date = 03/22/18 Pct Recovery = 72% Analysis Date = 03/22/18 Pct Recovery = 72% Analysis Date = 03/13/18 Pct Recovery = 72% Analysis Date = 03/13/18 Pct Recovery = 72% Analysis Date = 03/03/18 Pct Recovery = 72% Analysis Date = 03/03/18 Pct Recovery = 72% Analysis Date = 02/21/18 Pct Recovery = 72% Analysis Date = 02/21/18 Pct Recovery = 72% Analysis Date = 02/11/18 Pct Recovery = 72% Analysis Date = 02/11/18 Pct Recovery = 72% Analysis Date = 02/01/18 Pct Recovery = 72% Analysis Date = 02/01/18 Pct Recovery = 72% Analysis Date = 01/22/18 Pct Recovery = 72% Analysis Date = 01/22/18 Pct Recovery = 72% Analysis Date = 01/12/18 Pct Recovery = 71% Analysis Date = 01/12/18 Pct Recovery = 71% Analysis Date = 01/02/18 Pct Recovery = 71% Analysis Date = 01/02/18 Pct Recovery = 71% Analysis Date = 12/23/17 Pct Recovery = 71% Analysis Date = 12/23/17 Pct Recovery = 71% Analysis Date = 12/13/17 Pct Recovery = 71% Analysis Date = 12/13/17 Pct Recovery = 71% Analysis Date = 12/04/17 Pct Recovery = 71% Analysis Date = 12/04/17 Pct Recovery = 71% Analysis Date = 11/24/17 Pct Recovery = 71% Analysis Date = 11/24/17 Pct Recovery = 71% Analysis Date = 11/14/17 Pct Recovery = 71% Analysis Date = 11/14/17 Pct Recovery = 71% Analysis Date = 11/04/17 Pct Recovery = 71% Analysis Date = 11/04/17 Pct Recovery = 71% Analysis Date = 10/25/17 Pct Recovery = 71% Analysis Date = 10/25/17 Pct Recovery = 71% Analysis Date = 10/15/17 Pct Recovery = 71% Analysis Date = 10/15/17 Pct Recovery = 71% Analysis Date = 10/05/17 Pct Recovery = 71% Analysis Date = 10/05/17 Pct Recovery = 71% Analysis Date = 09/25/17 Pct Recovery = 71% Analysis Date = 09/25/17 Pct Recovery = 71% Analysis Date = 09/15/17 Pct Recovery = 71% Analysis Date = 09/15/17 Pct Recovery = 71% Analysis Date = 09/05/17 Pct Recovery = 71% Analysis Date = 09/05/17 Pct Recovery = 71% Analysis Date = 08/27/17 Pct Recovery = 71% Analysis Date = 08/27/17 Pct Recovery = 71% Analysis Date = 08/17/17 Pct Recovery = 71% Analysis Date = 08/17/17 Pct Recovery = 71% Analysis Date = 08/07/17 Pct Recovery = 71% Analysis Date = 08/07/17 Pct Recovery = 71% Analysis Date = 07/28/17 Pct Recovery = 70% Analysis Date = 07/28/17 Pct Recovery = 70% Analysis Date = 07/18/17 Pct Recovery = 70% Analysis Date = 07/18/17 Pct Recovery = 70% Analysis Date = 07/08/17 Pct Recovery = 70% Analysis Date = 07/08/17 Pct Recovery = 70% Analysis Date = 06/28/17 Pct Recovery = 70% Analysis Date = 06/28/17 Pct Recovery = 70% Analysis Date = 06/18/17 Pct Recovery = 70% Analysis Date = 06/18/17 Pct Recovery = 70% Analysis Date = 06/08/17 Pct Recovery = 70% Analysis Date = 06/08/17 Pct Recovery = 70% Analysis Date = 05/29/17 Pct Recovery = 70% Analysis Date = 05/29/17 Pct Recovery = 70% Analysis Date = 05/20/17 Pct Recovery = 70% Analysis Date = 05/20/17 Pct Recovery = 70% Analysis Date = 05/10/17 Pct Recovery = 70% Analysis Date = 05/10/17 Pct Recovery = 70% Analysis Date = 04/30/17 Pct Recovery = 70% Analysis Date = 04/30/17 Pct Recovery = 70% Analysis Date = 04/20/17 Pct Recovery = 70% Analysis Date = 04/20/17 Pct Recovery = 70% Analysis Date = 04/10/17 Pct Recovery = 70% Analysis Date = 04/10/17 Pct Recovery = 70% Analysis Date = 03/31/17 Pct Recovery = 70% Analysis Date = 03/31/17 Pct Recovery = 70% Analysis Date = 03/21/17 Pct Recovery = 70% Analysis Date = 03/21/17 Pct Recovery = 70% Analysis Date = 03/11/17 Pct Recovery = 70% Analysis Date = 03/11/17 Pct Recovery = 70% Analysis Date = 03/01/17 Pct Recovery = 70% Analysis Date = 03/01/17 Pct Recovery = 70% Analysis Date = 02/19/17 Pct Recovery = 70% Analysis Date = 02/19/17 Pct Recovery = 70% Analysis Date = 02/10/17 Pct Recovery = 70% Analysis Date = 02/10/17 Pct Recovery = 70% Analysis Date = 01/31/17 Pct Recovery = 70% Analysis Date = 01/31/17 Pct Recovery = 70% Analysis Date = 01/21/17 Pct Recovery = 69% Analysis Date = 01/21/17 Pct Recovery = 69% Analysis Date = 01/11/17 Pct Recovery = 69% Analysis Date = 01/11/17 Pct Recovery = 69% Analysis Date = 01/01/17 Pct Recovery = 69% Analysis Date = 01/01/17 Pct Recovery = 69% Analysis Date = 12/22/16 Pct Recovery = 69% Analysis Date = 12/22/16 Pct Recovery = 69% Analysis Date = 12/12/16 Pct Recovery = 69% Analysis Date = 12/12/16 Pct Recovery = 69% Analysis Date = 12/02/16 Pct Recovery = 69% Analysis Date = 12/02/16 Pct Recovery = 69% Analysis Date = 11/22/16 Pct Recovery = 69% Analysis Date = 11/22/16 Pct Recovery = 69% Analysis Date = 11/12/16 Pct Recovery = 69% Analysis Date = 11/12/16 Pct Recovery = 69% Analysis Date = 11/03/16 Pct Recovery = 69% Analysis Date = 11/03/16 Pct Recovery = 69% Analysis Date = 10/24/16 Pct Recovery = 69% Analysis Date = 10/24/16 Pct Recovery = 69% Analysis Date = 10/14/16 Pct Recovery = 69% Analysis Date = 10/14/16 Pct Recovery = 69% Analysis Date = 10/04/16 Pct Recovery = 69% Analysis Date = 10/04/16 Pct Recovery = 69% Analysis Date = 09/24/16 Pct Recovery = 69% Analysis Date = 09/24/16 Pct Recovery = 69% Analysis Date = 09/14/16 Pct Recovery = 69% Analysis Date = 09/14/16 Pct Recovery = 69% Analysis Date = 09/04/16 Pct Recovery = 69% Analysis Date = 09/04/16 Pct Recovery = 69% Analysis Date = 08/25/16 Pct Recovery = 69% Analysis Date = 08/25/16 Pct Recovery = 69% Analysis Date = 08/15/16 Pct Recovery = 68% Analysis Date = 08/15/16 Pct Recovery = 68% Analysis Date = 08/05/16 Pct Recovery = 68% Analysis Date = 08/05/16 Pct Recovery = 68% Analysis Date = 07/27/16 Pct Recovery = 68% Analysis Date = 07/27/16 Pct Recovery = 68% Analysis Date = 07/17/16 Pct Recovery = 68% Analysis Date = 07/17/16 Pct Recovery = 68% Analysis Date = 07/07/16 Pct Recovery = 68% Analysis Date = 07/07/16 Pct Recovery = 68% Analysis Date = 06/27/16 Pct Recovery = 68% Analysis Date = 06/27/16 Pct Recovery = 68% Analysis Date = 06/17/16 Pct Recovery = 68% Analysis Date = 06/17/16 Pct Recovery = 68% Analysis Date = 06/07/16 Pct Recovery = 68% Analysis Date = 06/07/16 Pct Recovery = 68% Analysis Date = 05/28/16 Pct Recovery = 67% Analysis Date = 05/28/16 Pct Recovery = 67% Analysis Date = 05/18/16 Pct Recovery = 67% Analysis Date = 05/18/16 Pct Recovery = 67% Analysis Date = 05/08/16 Pct Recovery = 67% Analysis Date = 05/08/16 Pct Recovery = 67% Analysis Date = 04/28/16 Pct Recovery = 67% Analysis Date = 04/28/16 Pct Recovery = 67% Analysis Date = 04/19/16 Pct Recovery = 67% Analysis Date = 04/19/16 Pct Recovery = 67% Analysis Date = 04/09/16 Pct Recovery = 67% Analysis Date = 04/09/16 Pct Recovery = 67% Analysis Date = 03/30/16 Pct Recovery = 67% Analysis Date = 03/30/16 Pct Recovery = 67% Analysis Date = 03/20/16 Pct Recovery = 66% Analysis Date = 03/20/16 Pct Recovery = 66% Analysis Date = 03/10/16 Pct Recovery = 66% Analysis Date = 03/10/16 Pct Recovery = 66% Analysis Date = 02/29/16 Pct Recovery = 66% Analysis Date = 02/29/16 Pct Recovery = 66% Analysis Date = 02/19/16 Pct Recovery = 66% Analysis Date = 02/19/16 Pct Recovery = 66% Analysis Date = 02/09/16 Pct Recovery = 66% Analysis Date = 02/09/16 Pct Recovery = 66% Analysis Date = 01/30/16 Pct Recovery = 66% Analysis Date = 01/30/16 Pct Recovery = 66% Analysis Date = 01/20/16 Pct Recovery = 66% Analysis Date = 01/20/16 Pct Recovery = 66% Analysis Date = 01/11/16 Pct Recovery = 66% Analysis Date = 01/11/16 Pct Recovery = 66% Analysis Date = 01/01/16 Pct Recovery = 66% Analysis Date = 01/01/16 Pct Recovery = 66% Analysis Date = 12/22/15 Pct Recovery = 66% Analysis Date = 12/22/15 Pct Recovery = 66% Analysis Date = 12/12/15 Pct Recovery = 66% Analysis Date = 12/12/15 Pct Recovery = 66% Analysis Date = 12/02/15 Pct Recovery = 66% Analysis Date = 12/02/15 Pct Recovery = 66% Analysis Date = 11/22/15 Pct Recovery = 66% Analysis Date = 11/22/15 Pct Recovery = 66% Analysis Date = 11/12/15 Pct Recovery = 66% Analysis Date = 11/12/15 Pct Recovery = 66% Analysis Date = 11/02/15 Pct Recovery = 66% Analysis Date = 11/02/15 Pct Recovery = 66% Analysis Date = 10/23/15 Pct Recovery = 66% Analysis Date = 10/23/15 Pct Recovery = 66% Analysis Date = 10/13/15 Pct Recovery = 66% Analysis Date = 10/13/15 Pct Recovery = 66% Analysis Date = 10/04/15 Pct Recovery = 66% Analysis Date = 10/04/15 Pct Recovery = 66% Analysis Date = 09/24/15 Pct Recovery = 66% Analysis Date = 09/24/15 Pct Recovery = 66% Analysis Date = 09/14/15 Pct Recovery = 66% Analysis Date = 09/14/15 Pct Recovery = 66% Analysis Date = 09/04/15 Pct Recovery = 66% Analysis Date = 09/04/15 Pct Recovery = 66% Analysis Date = 08/25/15 Pct Recovery = 66% Analysis Date = 08/25/15 Pct Recovery = 66% Analysis Date = 08/15/15 Pct Recovery = 67% Analysis Date = 08/15/15 Pct Recovery = 67% Analysis Date = 08/05/15 Pct Recovery = 67% Analysis Date = 08/05/15 Pct Recovery = 67% Analysis Date = 07/26/15 Pct Recovery = 67% Analysis Date = 07/26/15 Pct Recovery = 67% Analysis Date = 07/16/15 Pct Recovery = 67% Analysis Date = 07/16/15 Pct Recovery = 67% Analysis Date = 07/06/15 Pct Recovery = 67% Analysis Date = 07/06/15 Pct Recovery = 67% Analysis Date = 06/27/15 Pct Recovery = 67% Analysis Date = 06/27/15 Pct Recovery = 67% Analysis Date = 06/17/15 Pct Recovery = 67% Analysis Date = 06/17/15 Pct Recovery = 67% Analysis Date = 06/07/15 Pct Recovery = 68% Analysis Date = 06/07/15 Pct Recovery = 68% Analysis Date = 05/28/15 Pct Recovery = 68% Analysis Date = 05/28/15 Pct Recovery = 68% Analysis Date = 05/18/15 Pct Recovery = 68% Analysis Date = 05/18/15 Pct Recovery = 68% Analysis Date = 05/08/15 Pct Recovery = 68% Analysis Date = 05/08/15 Pct Recovery = 68% Analysis Date = 04/28/15 Pct Recovery = 68% Analysis Date = 04/28/15 Pct Recovery = 68% Analysis Date = 04/18/15 Pct Recovery = 69% Analysis Date = 04/18/15 Pct Recovery = 69% Analysis Date = 04/08/15 Pct Recovery = 69% Analysis Date = 04/08/15 Pct Recovery = 69% Analysis Date = 03/29/15 Pct Recovery = 69% Analysis Date = 03/29/15 Pct Recovery = 69% Analysis Date = 03/20/15 Pct Recovery = 70% Analysis Date = 03/20/15 Pct Recovery = 70% Analysis Date = 03/10/15 Pct Recovery = 70% Analysis Date = 03/10/15 Pct Recovery = 70% Analysis Date = 02/28/15 Pct Recovery = 70% Analysis Date = 02/28/15 Pct Recovery = 70% Analysis Date = 02/18/15 Pct Recovery = 71% Analysis Date = 02/18/15 Pct Recovery = 71% Analysis Date = 02/08/15 Pct Recovery = 71% Analysis Date = 02/08/15 Pct Recovery = 71% Analysis Date = 01/29/15 Pct Recovery = 71% Analysis Date = 01/29/15 Pct Recovery = 71% Analysis Date = 01/19/15 Pct Recovery = 72% Analysis Date = 01/19/15 Pct Recovery = 72% Analysis Date = 01/09/15 Pct Recovery = 72% Analysis Date = 01/09/15 Pct Recovery = 72% Analysis Date = 12/30/14 Pct Recovery = 72% Analysis Date = 12/30/14 Pct Recovery = 72% Analysis Date = 12/20/14 Pct Recovery = 72% Analysis Date = 12/20/14 Pct Recovery = 72% Analysis Date = 12/11/14 Pct Recovery = 73% Analysis Date = 12/11/14 Pct Recovery = 73% Analysis Date = 12/01/14 Pct Recovery = 73% Analysis Date = 12/01/14 Pct Recovery = 73% Analysis Date = 11/21/14 Pct Recovery = 73% Analysis Date = 11/21/14 Pct Recovery = 73% Analysis Date = 11/11/14 Pct Recovery = 73% Analysis Date = 11/11/14 Pct Recovery = 73% Analysis Date = 11/01/14 Pct Recovery = 74% Analysis Date = 11/01/14 Pct Recovery = 74% Analysis Date = 10/22/14 Pct Recovery = 74% Analysis Date = 10/22/14 Pct Recovery = 74% Analysis Date = 10/12/14 Pct Recovery = 74% Analysis Date = 10/12/14 Pct Recovery = 74% Analysis Date = 10/02/14 Pct Recovery = 74% Analysis Date = 10/02/14 Pct Recovery = 74% Analysis Date = 09/22/14 Pct Recovery = 75% Analysis Date = 09/22/14 Pct Recovery = 75% Analysis Date = 09/12/14 Pct Recovery = 75% Analysis Date = 09/12/14 Pct Recovery = 75% Analysis Date = 09/03/14 Pct Recovery = 75% Analysis Date = 09/03/14 Pct Recovery = 75% Analysis Date = 08/24/14 Pct Recovery = 75% Analysis Date = 08/24/14 Pct Recovery = 75% Analysis Date = 08/14/14 Pct Recovery = 76% Analysis Date = 08/14/14 Pct Recovery = 76% Analysis Date = 08/04/14 Pct Recovery = 76% Analysis Date = 08/04/14 Pct Recovery = 76% Analysis Date = 07/25/14 Pct Recovery = 76% Analysis Date = 07/25/14 Pct Recovery = 76% Analysis Date = 07/15/14 Pct Recovery = 76% Analysis Date = 07/15/14 Pct Recovery = 76% Analysis Date = 07/05/14 Pct Recovery = 77% Analysis Date = 07/05/14 Pct Recovery = 77% Analysis Date = 06/25/14 Pct Recovery = 77% Analysis Date = 06/25/14 Pct Recovery = 77% Analysis Date = 06/15/14 Pct Recovery = 77% Analysis Date = 06/15/14 Pct Recovery = 77% Analysis Date = 06/05/14 Pct Recovery = 77% Analysis Date = 06/05/14 Pct Recovery = 77% Analysis Date = 05/27/14 Pct Recovery = 78% Analysis Date = 05/27/14 Pct Recovery = 78% Analysis Date = 05/17/14 Pct Recovery = 78% Analysis Date = 05/17/14 Pct Recovery = 78% Analysis Date = 05/07/14 Pct Recovery = 78% Analysis Date = 05/07/14 Pct Recovery = 78% Analysis Date = 04/27/14 Pct Recovery = 78% Analysis Date = 04/27/14 Pct Recovery = 78% Analysis Date = 04/17/14 Pct Recovery = 78% Analysis Date = 04/17/14 Pct Recovery = 78% Analysis Date = 04/07/14 Pct Recovery = 79% Analysis Date = 04/07/14 Pct Recovery = 79% Analysis Date = 03/28/14 Pct Recovery = 79% Analysis Date = 03/28/14 Pct Recovery = 79% Analysis Date = 03/18/14 Pct Recovery = 79% Analysis Date = 03/18/14 Pct Recovery = 79% Analysis Date = 03/08/14 Pct Recovery = 79% Analysis Date = 03/08/14 Pct Recovery = 79% Analysis Date = 02/26/14 Pct Recovery = 80% Analysis Date = 02/26/14 Pct Recovery = 80% Analysis Date = 02/17/14 Pct Recovery = 80% Analysis Date = 02/17/14 Pct Recovery = 80% Analysis Date = 02/07/14 Pct Recovery = 80% Analysis Date = 02/07/14 Pct Recovery = 80% Analysis Date = 01/28/14 Pct Recovery = 80% Analysis Date = 01/28/14 Pct Recovery = 80% Analysis Date = 01/18/14 Pct Recovery = 81% Analysis Date = 01/18/14 Pct Recovery = 81% Analysis Date = 01/08/14 Pct Recovery = 81% Analysis Date = 01/08/14 Pct Recovery = 81% Analysis Date = 12/29/13 Pct Recovery = 81% Analysis Date = 12/29/13 Pct Recovery = 81% Analysis Date = 12/19/13 Pct Recovery = 81% Analysis Date = 12/19/13 Pct Recovery = 81% Analysis Date = 12/09/13 Pct Recovery = 81% Analysis Date = 12/09/13 Pct Recovery = 81% Analysis Date = 11/29/13 Pct Recovery = 82% Analysis Date = 11/29/13 Pct Recovery = 82% Analysis Date = 11/19/13 Pct Recovery = 82% Analysis Date = 11/19/13 Pct Recovery = 82% Analysis Date = 11/10/13 Pct Recovery = 82% Analysis Date = 11/10/13 Pct Recovery = 82% Analysis Date = 10/31/13 Pct Recovery = 82% Analysis Date = 10/31/13 Pct Recovery = 82% Analysis Date = 10/21/13 Pct Recovery = 83% Analysis Date = 10/21/13 Pct Recovery = 83% Analysis Date = 10/11/13 Pct Recovery = 83% Analysis Date = 10/11/13 Pct Recovery = 83% Analysis Date = 10/01/13 Pct Recovery = 83% Analysis Date = 10/01/13 Pct Recovery = 83% Analysis Date = 09/21/13 Pct Recovery = 83% Analysis Date = 09/21/13 Pct Recovery = 83% Analysis Date = 09/11/13 Pct Recovery = 83% Analysis Date = 09/11/13 Pct Recovery = 83% Analysis Date = 09/01/13 Pct Recovery = 84% Analysis Date = 09/01/13 Pct Recovery = 84% Analysis Date = 08/22/13 Pct Recovery = 84% Analysis Date = 08/22/13 Pct Recovery = 84% Analysis Date = 08/12/13 Pct Recovery = 84% Analysis Date = 08/12/13 Pct Recovery = 84% Analysis Date = 08/03/13 Pct Recovery = 84% Analysis Date = 08/03/13 Pct Recovery = 84% Analysis Date = 07/24/13 Pct Recovery = 85% Analysis Date = 07/24/13 Pct Recovery = 85% Analysis Date = 07/14/13 Pct Recovery = 85% Analysis Date = 07/14/13 Pct Recovery = 85% Analysis Date = 07/04/13 Pct Recovery = 85% Analysis Date = 07/04/13 Pct Recovery = 85% Analysis Date = 06/24/13 Pct Recovery = 85% Analysis Date = 06/24/13 Pct Recovery = 85% Analysis Date = 06/14/13 Pct Recovery = 85% Analysis Date = 06/14/13 Pct Recovery = 85% Analysis Date = 06/04/13 Pct Recovery = 86% Analysis Date = 06/04/13 Pct Recovery = 86% Analysis Date = 05/25/13 Pct Recovery = 86% Analysis Date = 05/25/13 Pct Recovery = 86% Analysis Date = 05/15/13 Pct Recovery = 86% Analysis Date = 05/15/13 Pct Recovery = 86% Analysis Date = 05/05/13 Pct Recovery = 86% Analysis Date = 05/05/13 Pct Recovery = 86% Analysis Date = 04/26/13 Pct Recovery = 87% Analysis Date = 04/26/13 Pct Recovery = 87% Analysis Date = 04/16/13 Pct Recovery = 87% Analysis Date = 04/16/13 Pct Recovery = 87% Analysis Date = 04/06/13 Pct Recovery = 87% Analysis Date = 04/06/13 Pct Recovery = 87% Analysis Date = 03/27/13 Pct Recovery = 87% Analysis Date = 03/27/13 Pct Recovery = 87% Analysis Date = 03/17/13 Pct Recovery = 87% Analysis Date = 03/17/13 Pct Recovery = 87% Analysis Date = 03/07/13 Pct Recovery = 88% Analysis Date = 03/07/13 Pct Recovery = 88% Analysis Date = 02/25/13 Pct Recovery = 88% Analysis Date = 02/25/13 Pct Recovery = 88% Analysis Date = 02/15/13 Pct Recovery = 88% Analysis Date = 02/15/13 Pct Recovery = 88% Analysis Date = 02/05/13 Pct Recovery = 88% Analysis Date = 02/05/13 Pct Recovery = 88% Analysis Date = 01/26/13 Pct Recovery = 89% Analysis Date = 01/26/13 Pct Recovery = 89% Analysis Date = 01/17/13 Pct Recovery = 89% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
CARBARYL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 82 74% 16% 74% 18%
Total 82 74% 16% 74% 18%

Sample Statistics
CARBARYL

Characteristic N % % Basis
Plotted 82 100% Spiked
Estimated Values 82 100% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 82 .  
False Negatives 0 0% 0 out of 82
Not Spiked 52 .  
False Positives 3 6% 3 out of 52

OBSP Determination:
CARBOFURAN
METHOD: 2033 , TESTIDCODE: 82674GCM35

Laboratory ID = 20130250061 Lab Value = 0.409 Expected Conc. = 0.498 Report level label = 0.06 Pct Recovery = 82% Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl SpecificMix = 05BB029 Laboratory ID = 20140100085 Lab Value = 0.440 Expected Conc. = 0.451 Report level label = 0.06 Pct Recovery = 98% Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl SpecificMix = 042413 Laboratory ID = 20180390003 Lab Value = 0.277 Expected Conc. = 0.402 Report level label = 0.06 Pct Recovery = 69% Analysis Date = 04/06/18 SpikeMix = Spex Organics EN170808006: 100 µl & Abs 071717Pest: 100 µl SpecificMix = 071717Pest Laboratory ID = 20172510330 Lab Value = 0.302 Expected Conc. = 0.398 Report level label = 0.06 Pct Recovery = 76% Analysis Date = 12/29/17 SpikeMix = ChemService 6537100: 100 µl & Abs 071817Pest: 100 µl SpecificMix = 6537100 Laboratory ID = 20162860079 Lab Value = 0.295 Expected Conc. = 0.371 Report level label = 0.06 Pct Recovery = 80% Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl SpecificMix = 060916 Laboratory ID = 20163150006 Lab Value = 0.305 Expected Conc. = 0.371 Report level label = 0.06 Pct Recovery = 82% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl SpecificMix = 060916 Laboratory ID = 20152750006 Lab Value = 0.281 Expected Conc. = 0.36 Report level label = 0.06 Pct Recovery = 78% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl SpecificMix = 040615 Laboratory ID = 20152610011 Lab Value = 0.116 Expected Conc. = 0.36 Report level label = 0.06 Pct Recovery = 32% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl SpecificMix = 040615 Laboratory ID = 20171380001 Lab Value = 0.178 Expected Conc. = 0.3032 Report level label = 0.06 Pct Recovery = 59% Analysis Date = 06/07/17 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 041816 Laboratory ID = 20170740063 Lab Value = 0.091 Expected Conc. = 0.3032 Report level label = 0.06 Pct Recovery = 30% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl SpecificMix = 041816 Laboratory ID = 20161740258 Lab Value = 0.175 Expected Conc. = 0.3032 Report level label = 0.06 Pct Recovery = 58% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 041816 Laboratory ID = 20171660002 Lab Value = 0.291 Expected Conc. = 0.2968 Report level label = 0.06 Pct Recovery = 98% Analysis Date = 08/23/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = 060916 Laboratory ID = 20170190026 Lab Value = 0.230 Expected Conc. = 0.2968 Report level label = 0.06 Pct Recovery = 77% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = 060916 Laboratory ID = 20130940097 Lab Value = 0.193 Expected Conc. = 0.252 Report level label = 0.06 Pct Recovery = 77% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = 052412 Laboratory ID = 20130100066 Lab Value = 0.257 Expected Conc. = 0.252 Report level label = 0.06 Pct Recovery = 102% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl SpecificMix = 052412 Laboratory ID = 20140230082 Lab Value = 0.193 Expected Conc. = 0.2505 Report level label = 0.06 Pct Recovery = 77% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl SpecificMix = 012513 Laboratory ID = 20132420001 Lab Value = 0.202 Expected Conc. = 0.2505 Report level label = 0.06 Pct Recovery = 81% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl SpecificMix = 012513 Laboratory ID = 20150720069 Lab Value = 0.103 Expected Conc. = 0.2406 Report level label = 0.06 Pct Recovery = 43% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 0227-14-08 Laboratory ID = 20141770149 Lab Value = 0.169 Expected Conc. = 0.2406 Report level label = 0.06 Pct Recovery = 70% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl SpecificMix = 0227-14-08 Laboratory ID = 20141570088 Lab Value = 0.234 Expected Conc. = 0.2406 Report level label = 0.06 Pct Recovery = 97% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl SpecificMix = 0227-14-08 Laboratory ID = 20150430092 Lab Value = 0.090 Expected Conc. = 0.2376 Report level label = 0.06 Pct Recovery = 38% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl SpecificMix = 042814 Laboratory ID = 20143240095 Lab Value = 0.229 Expected Conc. = 0.2376 Report level label = 0.06 Pct Recovery = 96% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl SpecificMix = 042814 Laboratory ID = 20142960086 Lab Value = 0.161 Expected Conc. = 0.2376 Report level label = 0.06 Pct Recovery = 68% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 042814 Laboratory ID = 20142530087 Lab Value = 0.164 Expected Conc. = 0.2376 Report level label = 0.06 Pct Recovery = 69% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl SpecificMix = 042814 Laboratory ID = 20132690010 Lab Value = 0.251 Expected Conc. = 0.2255 Report level label = 0.06 Pct Recovery = 111% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl SpecificMix = 042413 Laboratory ID = 20132560001 Lab Value = 0.211 Expected Conc. = 0.2255 Report level label = 0.06 Pct Recovery = 94% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl SpecificMix = 042413 Laboratory ID = 20132140002 Lab Value = 0.188 Expected Conc. = 0.224 Report level label = 0.06 Pct Recovery = 84% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl SpecificMix = 04CC101 Laboratory ID = 20173480003 Lab Value = 0.155 Expected Conc. = 0.201 Report level label = 0.06 Pct Recovery = 77% Analysis Date = 04/05/18 SpikeMix = Abs 071717Pest: 50 µl & ChemService 6567600: 50 µl SpecificMix = 071717Pest Laboratory ID = 20172230001 Lab Value = 0.218 Expected Conc. = 0.201 Report level label = 0.06 Pct Recovery = 108% Analysis Date = 10/19/17 SpikeMix = ChemService 6472100: 50 µl & Abs 071717Pest: 50 µl SpecificMix = 071717Pest Laboratory ID = 20172370001 Lab Value = 0.151 Expected Conc. = 0.199 Report level label = 0.06 Pct Recovery = 76% Analysis Date = 11/18/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6537100: 50 µl SpecificMix = 6537100 Laboratory ID = 20161260151 Lab Value = 0.123 Expected Conc. = 0.18 Report level label = 0.06 Pct Recovery = 68% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = EN150513008 Laboratory ID = 20160770090 Lab Value = 0.124 Expected Conc. = 0.18 Report level label = 0.06 Pct Recovery = 69% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = EN150513008 Laboratory ID = 20153510109 Lab Value = 0.114 Expected Conc. = 0.18 Report level label = 0.06 Pct Recovery = 63% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = EN150513008 Laboratory ID = 20152330039 Lab Value = 0.115 Expected Conc. = 0.18 Report level label = 0.06 Pct Recovery = 64% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl SpecificMix = EN150513008 Laboratory ID = 20151900132 Lab Value = 0.149 Expected Conc. = 0.18 Report level label = 0.06 Pct Recovery = 83% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl SpecificMix = 040615 Laboratory ID = 20151550293 Lab Value = 0.149 Expected Conc. = 0.18 Report level label = 0.06 Pct Recovery = 83% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl SpecificMix = 040615 Laboratory ID = 20172020035 Lab Value = 0.156 Expected Conc. = 0.1608 Report level label = 0.06 Pct Recovery = 97% Analysis Date = 11/07/17 SpikeMix = Abs 071717Pest: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 071717Pest Laboratory ID = 20171940002 Lab Value = 0.149 Expected Conc. = 0.1516 Report level label = 0.06 Pct Recovery = 98% Analysis Date = 11/10/17 SpikeMix = ChemService 5054800: 40 µl & NSI 041816: 40 µl SpecificMix = 041816 Laboratory ID = 20162020124 Lab Value = 0.114 Expected Conc. = 0.1516 Report level label = 0.06 Pct Recovery = 75% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl SpecificMix = 041816 Laboratory ID = 20161600087 Lab Value = 0.123 Expected Conc. = 0.1516 Report level label = 0.06 Pct Recovery = 81% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 041816 Laboratory ID = 20161340228 Lab Value = 0.110 Expected Conc. = 0.1516 Report level label = 0.06 Pct Recovery = 73% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl SpecificMix = 041816 Laboratory ID = 20161190075 Lab Value = 0.099 Expected Conc. = 0.1516 Report level label = 0.06 Pct Recovery = 65% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 041816 Laboratory ID = 20171160110 Lab Value = 0.111 Expected Conc. = 0.1484 Report level label = 0.06 Pct Recovery = 75% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = 060916 Laboratory ID = 20162520001 Lab Value = 0.143 Expected Conc. = 0.1484 Report level label = 0.06 Pct Recovery = 96% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl SpecificMix = 060916 Laboratory ID = 20163560019 Lab Value = 0.104 Expected Conc. = 0.1484 Report level label = 0.06 Pct Recovery = 70% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl SpecificMix = 060916 Laboratory ID = 20162380004 Lab Value = 0.144 Expected Conc. = 0.1484 Report level label = 0.06 Pct Recovery = 97% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = 060916 Laboratory ID = 20180940080 Lab Value = 0.100 Expected Conc. = 0.1206 Report level label = 0.06 Pct Recovery = 83% Analysis Date = 05/31/18 SpikeMix = ChemService 6472100: 30 µl & Abs 071717Pest: 30 µl SpecificMix = 071717Pest Laboratory ID = 20180730064 Lab Value = 0.135 Expected Conc. = 0.1206 Report level label = 0.06 Pct Recovery = 112% Analysis Date = 05/16/18 SpikeMix = Abs 071717Pest: 30 µl & Abs 071817Pest: 30 µl SpecificMix = 071717Pest Laboratory ID = 20141840097 Lab Value = 0.096 Expected Conc. = 0.1203 Report level label = 0.06 Pct Recovery = 80% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20141490205 Lab Value = 0.121 Expected Conc. = 0.1203 Report level label = 0.06 Pct Recovery = 101% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20141420140 Lab Value = 0.100 Expected Conc. = 0.1203 Report level label = 0.06 Pct Recovery = 83% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20141360094 Lab Value = 0.100 Expected Conc. = 0.1203 Report level label = 0.06 Pct Recovery = 83% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20173120093 Lab Value = 0.107 Expected Conc. = 0.1194 Report level label = 0.06 Pct Recovery = 90% Analysis Date = 03/10/18 SpikeMix = ChemService 6472100: 30 µl & ChemService 6537100: 30 µl SpecificMix = 6537100 Laboratory ID = 20172780018 Lab Value = 0.082 Expected Conc. = 0.1194 Report level label = 0.06 Pct Recovery = 68% Analysis Date = 02/08/18 SpikeMix = ChemService 6537100: 30 µl & Abs 071817Pest: 30 µl SpecificMix = 6537100 Laboratory ID = 20143370094 Lab Value = 0.080 Expected Conc. = 0.1188 Report level label = 0.06 Pct Recovery = 68% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl SpecificMix = 042814 Laboratory ID = 20142820151 Lab Value = 0.100 Expected Conc. = 0.1188 Report level label = 0.06 Pct Recovery = 84% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl SpecificMix = 042814 Laboratory ID = 20142470041 Lab Value = 0.113 Expected Conc. = 0.1188 Report level label = 0.06 Pct Recovery = 95% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl SpecificMix = 042814 Laboratory ID = 20142200164 Lab Value = 0.096 Expected Conc. = 0.1188 Report level label = 0.06 Pct Recovery = 81% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 042814 Laboratory ID = 20133400002 Lab Value = 0.107 Expected Conc. = 0.1008 Report level label = 0.06 Pct Recovery = 106% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = 052412 Laboratory ID = 20132910008 Lab Value = 0.084 Expected Conc. = 0.1008 Report level label = 0.06 Pct Recovery = 83% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = 052412 Laboratory ID = 20130650005 Lab Value = 0.075 Expected Conc. = 0.1008 Report level label = 0.06 Pct Recovery = 74% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl SpecificMix = 052412 Laboratory ID = 20140860102 Lab Value = 0.082 Expected Conc. = 0.1002 Report level label = 0.06 Pct Recovery = 82% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 012513 Laboratory ID = 20131920149 Lab Value = 0.092 Expected Conc. = 0.1002 Report level label = 0.06 Pct Recovery = 92% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl SpecificMix = 012513 Laboratory ID = 20131230084 Lab Value = 0.116 Expected Conc. = 0.0996 Report level label = 0.06 Pct Recovery = 116% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl SpecificMix = 05BB029 Laboratory ID = 20130510051 Lab Value = 0.091 Expected Conc. = 0.0996 Report level label = 0.06 Pct Recovery = 91% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl SpecificMix = 05BB029 Laboratory ID = 20133580036 Lab Value = 0.082 Expected Conc. = 0.0902 Report level label = 0.06 Pct Recovery = 91% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 042413 Laboratory ID = 20133190012 Lab Value = 0.096 Expected Conc. = 0.0902 Report level label = 0.06 Pct Recovery = 107% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 042413 Laboratory ID = 20131650073 Lab Value = 0.112 Expected Conc. = 0.0902 Report level label = 0.06 Pct Recovery = 124% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl SpecificMix = 042413 Laboratory ID = 20161050143 Lab Value = 0.077 Expected Conc. = 0.09 Report level label = 0.06 Pct Recovery = 86% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Laboratory ID = 20160430111 Lab Value = 0.081 Expected Conc. = 0.09 Report level label = 0.06 Pct Recovery = 90% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Laboratory ID = 20160560044 Lab Value = 0.057 Expected Conc. = 0.09 Report level label = 0.06 Pct Recovery = 64% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl SpecificMix = EN150513008 Laboratory ID = 20160070059 Lab Value = 0.067 Expected Conc. = 0.09 Report level label = 0.06 Pct Recovery = 75% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = 040615 Laboratory ID = 20153160001 Lab Value = 0.060 Expected Conc. = 0.09 Report level label = 0.06 Pct Recovery = 67% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = EN150513008 Laboratory ID = 20153030068 Lab Value = 0.068 Expected Conc. = 0.09 Report level label = 0.06 Pct Recovery = 76% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150513008 Laboratory ID = 20152190003 Lab Value = 0.059 Expected Conc. = 0.09 Report level label = 0.06 Pct Recovery = 66% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150513008 Laboratory ID = 20151480170 Lab Value = 0.065 Expected Conc. = 0.09 Report level label = 0.06 Pct Recovery = 72% Analysis Date = 06/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150513008 Laboratory ID = 20151380009 Lab Value = 0.082 Expected Conc. = 0.09 Report level label = 0.06 Pct Recovery = 91% Analysis Date = 05/30/15 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Laboratory ID = 20151210037 Lab Value = 0.085 Expected Conc. = 0.09 Report level label = 0.06 Pct Recovery = 95% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Laboratory ID = 20140730138 Lab Value = 0.051 Expected Conc. = 0.0896 Report level label = 0.06 Pct Recovery = 57% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 04CC101 Laboratory ID = 20140510043 Lab Value = 0.078 Expected Conc. = 0.0896 Report level label = 0.06 Pct Recovery = 87% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 04CC101 Laboratory ID = 20133310030 Lab Value = 0.095 Expected Conc. = 0.0896 Report level label = 0.06 Pct Recovery = 106% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl SpecificMix = 04CC101 Laboratory ID = 20132280016 Lab Value = 0.097 Expected Conc. = 0.0896 Report level label = 0.06 Pct Recovery = 109% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl SpecificMix = 04CC101 Laboratory ID = 20131510026 Lab Value = 0.079 Expected Conc. = 0.0896 Report level label = 0.06 Pct Recovery = 88% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl SpecificMix = 04CC101 Analysis Date = 05/30/18 Pct Recovery = 87% Analysis Date = 05/21/18 Pct Recovery = 87% Analysis Date = 05/21/18 Pct Recovery = 87% Analysis Date = 05/11/18 Pct Recovery = 87% Analysis Date = 05/11/18 Pct Recovery = 87% Analysis Date = 05/01/18 Pct Recovery = 87% Analysis Date = 05/01/18 Pct Recovery = 87% Analysis Date = 04/21/18 Pct Recovery = 86% Analysis Date = 04/21/18 Pct Recovery = 86% Analysis Date = 04/11/18 Pct Recovery = 86% Analysis Date = 04/11/18 Pct Recovery = 86% Analysis Date = 04/02/18 Pct Recovery = 86% Analysis Date = 04/02/18 Pct Recovery = 86% Analysis Date = 03/23/18 Pct Recovery = 86% Analysis Date = 03/23/18 Pct Recovery = 86% Analysis Date = 03/13/18 Pct Recovery = 86% Analysis Date = 03/13/18 Pct Recovery = 86% Analysis Date = 03/03/18 Pct Recovery = 85% Analysis Date = 03/03/18 Pct Recovery = 85% Analysis Date = 02/21/18 Pct Recovery = 85% Analysis Date = 02/21/18 Pct Recovery = 85% Analysis Date = 02/12/18 Pct Recovery = 85% Analysis Date = 02/12/18 Pct Recovery = 85% Analysis Date = 02/02/18 Pct Recovery = 85% Analysis Date = 02/02/18 Pct Recovery = 85% Analysis Date = 01/23/18 Pct Recovery = 85% Analysis Date = 01/23/18 Pct Recovery = 85% Analysis Date = 01/13/18 Pct Recovery = 84% Analysis Date = 01/13/18 Pct Recovery = 84% Analysis Date = 01/03/18 Pct Recovery = 84% Analysis Date = 01/03/18 Pct Recovery = 84% Analysis Date = 12/25/17 Pct Recovery = 84% Analysis Date = 12/25/17 Pct Recovery = 84% Analysis Date = 12/15/17 Pct Recovery = 84% Analysis Date = 12/15/17 Pct Recovery = 84% Analysis Date = 12/05/17 Pct Recovery = 84% Analysis Date = 12/05/17 Pct Recovery = 84% Analysis Date = 11/25/17 Pct Recovery = 83% Analysis Date = 11/25/17 Pct Recovery = 83% Analysis Date = 11/15/17 Pct Recovery = 83% Analysis Date = 11/15/17 Pct Recovery = 83% Analysis Date = 11/06/17 Pct Recovery = 83% Analysis Date = 11/06/17 Pct Recovery = 83% Analysis Date = 10/27/17 Pct Recovery = 83% Analysis Date = 10/27/17 Pct Recovery = 83% Analysis Date = 10/17/17 Pct Recovery = 83% Analysis Date = 10/17/17 Pct Recovery = 83% Analysis Date = 10/07/17 Pct Recovery = 82% Analysis Date = 10/07/17 Pct Recovery = 82% Analysis Date = 09/27/17 Pct Recovery = 82% Analysis Date = 09/27/17 Pct Recovery = 82% Analysis Date = 09/18/17 Pct Recovery = 82% Analysis Date = 09/18/17 Pct Recovery = 82% Analysis Date = 09/08/17 Pct Recovery = 82% Analysis Date = 09/08/17 Pct Recovery = 82% Analysis Date = 08/29/17 Pct Recovery = 82% Analysis Date = 08/29/17 Pct Recovery = 82% Analysis Date = 08/19/17 Pct Recovery = 81% Analysis Date = 08/19/17 Pct Recovery = 81% Analysis Date = 08/09/17 Pct Recovery = 81% Analysis Date = 08/09/17 Pct Recovery = 81% Analysis Date = 07/31/17 Pct Recovery = 81% Analysis Date = 07/31/17 Pct Recovery = 81% Analysis Date = 07/21/17 Pct Recovery = 81% Analysis Date = 07/21/17 Pct Recovery = 81% Analysis Date = 07/11/17 Pct Recovery = 81% Analysis Date = 07/11/17 Pct Recovery = 81% Analysis Date = 07/01/17 Pct Recovery = 81% Analysis Date = 07/01/17 Pct Recovery = 81% Analysis Date = 06/21/17 Pct Recovery = 80% Analysis Date = 06/21/17 Pct Recovery = 80% Analysis Date = 06/12/17 Pct Recovery = 80% Analysis Date = 06/12/17 Pct Recovery = 80% Analysis Date = 06/02/17 Pct Recovery = 80% Analysis Date = 06/02/17 Pct Recovery = 80% Analysis Date = 05/23/17 Pct Recovery = 80% Analysis Date = 05/23/17 Pct Recovery = 80% Analysis Date = 05/13/17 Pct Recovery = 80% Analysis Date = 05/13/17 Pct Recovery = 80% Analysis Date = 05/03/17 Pct Recovery = 79% Analysis Date = 05/03/17 Pct Recovery = 79% Analysis Date = 04/24/17 Pct Recovery = 79% Analysis Date = 04/24/17 Pct Recovery = 79% Analysis Date = 04/14/17 Pct Recovery = 79% Analysis Date = 04/14/17 Pct Recovery = 79% Analysis Date = 04/04/17 Pct Recovery = 79% Analysis Date = 04/04/17 Pct Recovery = 79% Analysis Date = 03/25/17 Pct Recovery = 79% Analysis Date = 03/25/17 Pct Recovery = 79% Analysis Date = 03/15/17 Pct Recovery = 78% Analysis Date = 03/15/17 Pct Recovery = 78% Analysis Date = 03/06/17 Pct Recovery = 78% Analysis Date = 03/06/17 Pct Recovery = 78% Analysis Date = 02/24/17 Pct Recovery = 78% Analysis Date = 02/24/17 Pct Recovery = 78% Analysis Date = 02/14/17 Pct Recovery = 78% Analysis Date = 02/14/17 Pct Recovery = 78% Analysis Date = 02/04/17 Pct Recovery = 78% Analysis Date = 02/04/17 Pct Recovery = 78% Analysis Date = 01/25/17 Pct Recovery = 77% Analysis Date = 01/25/17 Pct Recovery = 77% Analysis Date = 01/16/17 Pct Recovery = 77% Analysis Date = 01/16/17 Pct Recovery = 77% Analysis Date = 01/06/17 Pct Recovery = 77% Analysis Date = 01/06/17 Pct Recovery = 77% Analysis Date = 12/27/16 Pct Recovery = 77% Analysis Date = 12/27/16 Pct Recovery = 77% Analysis Date = 12/17/16 Pct Recovery = 77% Analysis Date = 12/17/16 Pct Recovery = 77% Analysis Date = 12/07/16 Pct Recovery = 76% Analysis Date = 12/07/16 Pct Recovery = 76% Analysis Date = 11/28/16 Pct Recovery = 76% Analysis Date = 11/28/16 Pct Recovery = 76% Analysis Date = 11/18/16 Pct Recovery = 76% Analysis Date = 11/18/16 Pct Recovery = 76% Analysis Date = 11/08/16 Pct Recovery = 76% Analysis Date = 11/08/16 Pct Recovery = 76% Analysis Date = 10/29/16 Pct Recovery = 76% Analysis Date = 10/29/16 Pct Recovery = 76% Analysis Date = 10/19/16 Pct Recovery = 76% Analysis Date = 10/19/16 Pct Recovery = 76% Analysis Date = 10/10/16 Pct Recovery = 75% Analysis Date = 10/10/16 Pct Recovery = 75% Analysis Date = 09/30/16 Pct Recovery = 75% Analysis Date = 09/30/16 Pct Recovery = 75% Analysis Date = 09/20/16 Pct Recovery = 75% Analysis Date = 09/20/16 Pct Recovery = 75% Analysis Date = 09/10/16 Pct Recovery = 75% Analysis Date = 09/10/16 Pct Recovery = 75% Analysis Date = 08/31/16 Pct Recovery = 75% Analysis Date = 08/31/16 Pct Recovery = 75% Analysis Date = 08/22/16 Pct Recovery = 74% Analysis Date = 08/22/16 Pct Recovery = 74% Analysis Date = 08/12/16 Pct Recovery = 74% Analysis Date = 08/12/16 Pct Recovery = 74% Analysis Date = 08/02/16 Pct Recovery = 74% Analysis Date = 08/02/16 Pct Recovery = 74% Analysis Date = 07/23/16 Pct Recovery = 74% Analysis Date = 07/23/16 Pct Recovery = 74% Analysis Date = 07/13/16 Pct Recovery = 74% Analysis Date = 07/13/16 Pct Recovery = 74% Analysis Date = 07/04/16 Pct Recovery = 74% Analysis Date = 07/04/16 Pct Recovery = 74% Analysis Date = 06/24/16 Pct Recovery = 73% Analysis Date = 06/24/16 Pct Recovery = 73% Analysis Date = 06/14/16 Pct Recovery = 73% Analysis Date = 06/14/16 Pct Recovery = 73% Analysis Date = 06/04/16 Pct Recovery = 73% Analysis Date = 06/04/16 Pct Recovery = 73% Analysis Date = 05/25/16 Pct Recovery = 73% Analysis Date = 05/25/16 Pct Recovery = 73% Analysis Date = 05/16/16 Pct Recovery = 73% Analysis Date = 05/16/16 Pct Recovery = 73% Analysis Date = 05/06/16 Pct Recovery = 73% Analysis Date = 05/06/16 Pct Recovery = 73% Analysis Date = 04/26/16 Pct Recovery = 72% Analysis Date = 04/26/16 Pct Recovery = 72% Analysis Date = 04/16/16 Pct Recovery = 72% Analysis Date = 04/16/16 Pct Recovery = 72% Analysis Date = 04/06/16 Pct Recovery = 72% Analysis Date = 04/06/16 Pct Recovery = 72% Analysis Date = 03/28/16 Pct Recovery = 72% Analysis Date = 03/28/16 Pct Recovery = 72% Analysis Date = 03/18/16 Pct Recovery = 72% Analysis Date = 03/18/16 Pct Recovery = 72% Analysis Date = 03/08/16 Pct Recovery = 72% Analysis Date = 03/08/16 Pct Recovery = 72% Analysis Date = 02/27/16 Pct Recovery = 72% Analysis Date = 02/27/16 Pct Recovery = 72% Analysis Date = 02/17/16 Pct Recovery = 72% Analysis Date = 02/17/16 Pct Recovery = 72% Analysis Date = 02/08/16 Pct Recovery = 72% Analysis Date = 02/08/16 Pct Recovery = 72% Analysis Date = 01/29/16 Pct Recovery = 72% Analysis Date = 01/29/16 Pct Recovery = 72% Analysis Date = 01/19/16 Pct Recovery = 72% Analysis Date = 01/19/16 Pct Recovery = 72% Analysis Date = 01/09/16 Pct Recovery = 72% Analysis Date = 01/09/16 Pct Recovery = 72% Analysis Date = 12/30/15 Pct Recovery = 72% Analysis Date = 12/30/15 Pct Recovery = 72% Analysis Date = 12/21/15 Pct Recovery = 72% Analysis Date = 12/21/15 Pct Recovery = 72% Analysis Date = 12/11/15 Pct Recovery = 72% Analysis Date = 12/11/15 Pct Recovery = 72% Analysis Date = 12/01/15 Pct Recovery = 72% Analysis Date = 12/01/15 Pct Recovery = 72% Analysis Date = 11/21/15 Pct Recovery = 72% Analysis Date = 11/21/15 Pct Recovery = 72% Analysis Date = 11/11/15 Pct Recovery = 72% Analysis Date = 11/11/15 Pct Recovery = 72% Analysis Date = 11/02/15 Pct Recovery = 73% Analysis Date = 11/02/15 Pct Recovery = 73% Analysis Date = 10/23/15 Pct Recovery = 73% Analysis Date = 10/23/15 Pct Recovery = 73% Analysis Date = 10/13/15 Pct Recovery = 73% Analysis Date = 10/13/15 Pct Recovery = 73% Analysis Date = 10/03/15 Pct Recovery = 73% Analysis Date = 10/03/15 Pct Recovery = 73% Analysis Date = 09/23/15 Pct Recovery = 73% Analysis Date = 09/23/15 Pct Recovery = 73% Analysis Date = 09/14/15 Pct Recovery = 73% Analysis Date = 09/14/15 Pct Recovery = 73% Analysis Date = 09/04/15 Pct Recovery = 73% Analysis Date = 09/04/15 Pct Recovery = 73% Analysis Date = 08/25/15 Pct Recovery = 73% Analysis Date = 08/25/15 Pct Recovery = 73% Analysis Date = 08/15/15 Pct Recovery = 73% Analysis Date = 08/15/15 Pct Recovery = 73% Analysis Date = 08/05/15 Pct Recovery = 73% Analysis Date = 08/05/15 Pct Recovery = 73% Analysis Date = 07/27/15 Pct Recovery = 73% Analysis Date = 07/27/15 Pct Recovery = 73% Analysis Date = 07/17/15 Pct Recovery = 73% Analysis Date = 07/17/15 Pct Recovery = 73% Analysis Date = 07/07/15 Pct Recovery = 73% Analysis Date = 07/07/15 Pct Recovery = 73% Analysis Date = 06/27/15 Pct Recovery = 73% Analysis Date = 06/27/15 Pct Recovery = 73% Analysis Date = 06/17/15 Pct Recovery = 73% Analysis Date = 06/17/15 Pct Recovery = 73% Analysis Date = 06/08/15 Pct Recovery = 73% Analysis Date = 06/08/15 Pct Recovery = 73% Analysis Date = 05/29/15 Pct Recovery = 74% Analysis Date = 05/29/15 Pct Recovery = 74% Analysis Date = 05/19/15 Pct Recovery = 74% Analysis Date = 05/19/15 Pct Recovery = 74% Analysis Date = 05/09/15 Pct Recovery = 74% Analysis Date = 05/09/15 Pct Recovery = 74% Analysis Date = 04/29/15 Pct Recovery = 74% Analysis Date = 04/29/15 Pct Recovery = 74% Analysis Date = 04/20/15 Pct Recovery = 74% Analysis Date = 04/20/15 Pct Recovery = 74% Analysis Date = 04/10/15 Pct Recovery = 75% Analysis Date = 04/10/15 Pct Recovery = 75% Analysis Date = 03/31/15 Pct Recovery = 75% Analysis Date = 03/31/15 Pct Recovery = 75% Analysis Date = 03/21/15 Pct Recovery = 75% Analysis Date = 03/21/15 Pct Recovery = 75% Analysis Date = 03/11/15 Pct Recovery = 75% Analysis Date = 03/11/15 Pct Recovery = 75% Analysis Date = 03/02/15 Pct Recovery = 75% Analysis Date = 03/02/15 Pct Recovery = 75% Analysis Date = 02/20/15 Pct Recovery = 75% Analysis Date = 02/20/15 Pct Recovery = 75% Analysis Date = 02/10/15 Pct Recovery = 76% Analysis Date = 02/10/15 Pct Recovery = 76% Analysis Date = 01/31/15 Pct Recovery = 76% Analysis Date = 01/31/15 Pct Recovery = 76% Analysis Date = 01/21/15 Pct Recovery = 76% Analysis Date = 01/21/15 Pct Recovery = 76% Analysis Date = 01/12/15 Pct Recovery = 76% Analysis Date = 01/12/15 Pct Recovery = 76% Analysis Date = 01/02/15 Pct Recovery = 76% Analysis Date = 01/02/15 Pct Recovery = 76% Analysis Date = 12/23/14 Pct Recovery = 76% Analysis Date = 12/23/14 Pct Recovery = 76% Analysis Date = 12/13/14 Pct Recovery = 77% Analysis Date = 12/13/14 Pct Recovery = 77% Analysis Date = 12/03/14 Pct Recovery = 77% Analysis Date = 12/03/14 Pct Recovery = 77% Analysis Date = 11/24/14 Pct Recovery = 77% Analysis Date = 11/24/14 Pct Recovery = 77% Analysis Date = 11/14/14 Pct Recovery = 78% Analysis Date = 11/14/14 Pct Recovery = 78% Analysis Date = 11/04/14 Pct Recovery = 78% Analysis Date = 11/04/14 Pct Recovery = 78% Analysis Date = 10/25/14 Pct Recovery = 79% Analysis Date = 10/25/14 Pct Recovery = 79% Analysis Date = 10/15/14 Pct Recovery = 79% Analysis Date = 10/15/14 Pct Recovery = 79% Analysis Date = 10/06/14 Pct Recovery = 79% Analysis Date = 10/06/14 Pct Recovery = 79% Analysis Date = 09/26/14 Pct Recovery = 80% Analysis Date = 09/26/14 Pct Recovery = 80% Analysis Date = 09/16/14 Pct Recovery = 80% Analysis Date = 09/16/14 Pct Recovery = 80% Analysis Date = 09/06/14 Pct Recovery = 80% Analysis Date = 09/06/14 Pct Recovery = 80% Analysis Date = 08/27/14 Pct Recovery = 81% Analysis Date = 08/27/14 Pct Recovery = 81% Analysis Date = 08/18/14 Pct Recovery = 81% Analysis Date = 08/18/14 Pct Recovery = 81% Analysis Date = 08/08/14 Pct Recovery = 82% Analysis Date = 08/08/14 Pct Recovery = 82% Analysis Date = 07/29/14 Pct Recovery = 82% Analysis Date = 07/29/14 Pct Recovery = 82% Analysis Date = 07/19/14 Pct Recovery = 82% Analysis Date = 07/19/14 Pct Recovery = 82% Analysis Date = 07/09/14 Pct Recovery = 83% Analysis Date = 07/09/14 Pct Recovery = 83% Analysis Date = 06/30/14 Pct Recovery = 83% Analysis Date = 06/30/14 Pct Recovery = 83% Analysis Date = 06/20/14 Pct Recovery = 84% Analysis Date = 06/20/14 Pct Recovery = 84% Analysis Date = 06/10/14 Pct Recovery = 84% Analysis Date = 06/10/14 Pct Recovery = 84% Analysis Date = 05/31/14 Pct Recovery = 84% Analysis Date = 05/31/14 Pct Recovery = 84% Analysis Date = 05/21/14 Pct Recovery = 85% Analysis Date = 05/21/14 Pct Recovery = 85% Analysis Date = 05/12/14 Pct Recovery = 85% Analysis Date = 05/12/14 Pct Recovery = 85% Analysis Date = 05/02/14 Pct Recovery = 85% Analysis Date = 05/02/14 Pct Recovery = 85% Analysis Date = 04/22/14 Pct Recovery = 86% Analysis Date = 04/22/14 Pct Recovery = 86% Analysis Date = 04/12/14 Pct Recovery = 86% Analysis Date = 04/12/14 Pct Recovery = 86% Analysis Date = 04/02/14 Pct Recovery = 86% Analysis Date = 04/02/14 Pct Recovery = 86% Analysis Date = 03/24/14 Pct Recovery = 86% Analysis Date = 03/24/14 Pct Recovery = 86% Analysis Date = 03/14/14 Pct Recovery = 87% Analysis Date = 03/14/14 Pct Recovery = 87% Analysis Date = 03/04/14 Pct Recovery = 87% Analysis Date = 03/04/14 Pct Recovery = 87% Analysis Date = 02/22/14 Pct Recovery = 87% Analysis Date = 02/22/14 Pct Recovery = 87% Analysis Date = 02/12/14 Pct Recovery = 88% Analysis Date = 02/12/14 Pct Recovery = 88% Analysis Date = 02/03/14 Pct Recovery = 88% Analysis Date = 02/03/14 Pct Recovery = 88% Analysis Date = 01/24/14 Pct Recovery = 88% Analysis Date = 01/24/14 Pct Recovery = 88% Analysis Date = 01/14/14 Pct Recovery = 89% Analysis Date = 01/14/14 Pct Recovery = 89% Analysis Date = 01/04/14 Pct Recovery = 89% Analysis Date = 01/04/14 Pct Recovery = 89% Analysis Date = 12/25/13 Pct Recovery = 89% Analysis Date = 12/25/13 Pct Recovery = 89% Analysis Date = 12/16/13 Pct Recovery = 90% Analysis Date = 12/16/13 Pct Recovery = 90% Analysis Date = 12/06/13 Pct Recovery = 90% Analysis Date = 12/06/13 Pct Recovery = 90% Analysis Date = 11/26/13 Pct Recovery = 90% Analysis Date = 11/26/13 Pct Recovery = 90% Analysis Date = 11/16/13 Pct Recovery = 90% Analysis Date = 11/16/13 Pct Recovery = 90% Analysis Date = 11/06/13 Pct Recovery = 91% Analysis Date = 11/06/13 Pct Recovery = 91% Analysis Date = 10/28/13 Pct Recovery = 91% Analysis Date = 10/28/13 Pct Recovery = 91% Analysis Date = 10/18/13 Pct Recovery = 91% Analysis Date = 10/18/13 Pct Recovery = 91% Analysis Date = 10/08/13 Pct Recovery = 92% Analysis Date = 10/08/13 Pct Recovery = 92% Analysis Date = 09/28/13 Pct Recovery = 92% Analysis Date = 09/28/13 Pct Recovery = 92% Analysis Date = 09/18/13 Pct Recovery = 92% Analysis Date = 09/18/13 Pct Recovery = 92% Analysis Date = 09/09/13 Pct Recovery = 92% Analysis Date = 09/09/13 Pct Recovery = 92% Analysis Date = 08/30/13 Pct Recovery = 93% Analysis Date = 08/30/13 Pct Recovery = 93% Analysis Date = 08/20/13 Pct Recovery = 93% Analysis Date = 08/20/13 Pct Recovery = 93% Analysis Date = 08/10/13 Pct Recovery = 93% Analysis Date = 08/10/13 Pct Recovery = 93% Analysis Date = 07/31/13 Pct Recovery = 94% Analysis Date = 07/31/13 Pct Recovery = 94% Analysis Date = 07/22/13 Pct Recovery = 94% Analysis Date = 07/22/13 Pct Recovery = 94% Analysis Date = 07/12/13 Pct Recovery = 94% Analysis Date = 07/12/13 Pct Recovery = 94% Analysis Date = 07/02/13 Pct Recovery = 94% Analysis Date = 07/02/13 Pct Recovery = 94% Analysis Date = 06/22/13 Pct Recovery = 95% Analysis Date = 06/22/13 Pct Recovery = 95% Analysis Date = 06/12/13 Pct Recovery = 95% Analysis Date = 06/12/13 Pct Recovery = 95% Analysis Date = 06/03/13 Pct Recovery = 95% Analysis Date = 06/03/13 Pct Recovery = 95% Analysis Date = 05/24/13 Pct Recovery = 96% Analysis Date = 05/24/13 Pct Recovery = 96% Analysis Date = 05/14/13 Pct Recovery = 96% Analysis Date = 05/14/13 Pct Recovery = 96% Analysis Date = 05/04/13 Pct Recovery = 96% Analysis Date = 05/04/13 Pct Recovery = 96% Analysis Date = 04/24/13 Pct Recovery = 96% Analysis Date = 04/24/13 Pct Recovery = 96% Analysis Date = 04/15/13 Pct Recovery = 97% Analysis Date = 04/15/13 Pct Recovery = 97% Analysis Date = 04/05/13 Pct Recovery = 97% Analysis Date = 04/05/13 Pct Recovery = 97% Analysis Date = 03/26/13 Pct Recovery = 97% Analysis Date = 03/26/13 Pct Recovery = 97% Analysis Date = 03/16/13 Pct Recovery = 97% Analysis Date = 03/16/13 Pct Recovery = 97% Analysis Date = 03/06/13 Pct Recovery = 98% Analysis Date = 03/06/13 Pct Recovery = 98% Analysis Date = 02/25/13 Pct Recovery = 98% Analysis Date = 02/25/13 Pct Recovery = 98% Analysis Date = 02/15/13 Pct Recovery = 98% Analysis Date = 02/15/13 Pct Recovery = 98% Analysis Date = 02/05/13 Pct Recovery = 98% Analysis Date = 02/05/13 Pct Recovery = 98% Analysis Date = 01/26/13 Pct Recovery = 99% Analysis Date = 01/26/13 Pct Recovery = 99% Analysis Date = 01/17/13 Pct Recovery = 99% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
CARBOFURAN

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 83 82% 18% 82% 18%
Total 83 82% 18% 82% 18%

Sample Statistics
CARBOFURAN

Characteristic N % % Basis
Plotted 83 100% Spiked
Estimated Values 83 100% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 83 .  
False Negatives 0 0% 0 out of 83
Not Spiked 51 .  
False Positives 0 0% 0 out of 51

OBSP Determination:
CHLORPYRIFOS
METHOD: 2033 , TESTIDCODE: 38933GCM35

Laboratory ID = 20130250061 Lab Value = 0.436 Expected Conc. = 0.498 Report level label = 0.01 Pct Recovery = 88% Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl SpecificMix = 05BB029 Laboratory ID = 20140230082 Lab Value = 0.199 Expected Conc. = 0.2505 Report level label = 0.01 Pct Recovery = 79% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl SpecificMix = 012513 Laboratory ID = 20132420001 Lab Value = 0.228 Expected Conc. = 0.2505 Report level label = 0.01 Pct Recovery = 91% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl SpecificMix = 012513 Laboratory ID = 20130940097 Lab Value = 0.194 Expected Conc. = 0.2505 Report level label = 0.01 Pct Recovery = 77% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = 052412 Laboratory ID = 20130100066 Lab Value = 0.245 Expected Conc. = 0.2505 Report level label = 0.01 Pct Recovery = 98% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl SpecificMix = 052412 Laboratory ID = 20140100085 Lab Value = 0.174 Expected Conc. = 0.19 Report level label = 0.01 Pct Recovery = 92% Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl SpecificMix = T1130514013 Laboratory ID = 20132490342 Lab Value = 0.213 Expected Conc. = 0.19 Report level label = 0.01 Pct Recovery = 112% Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl SpecificMix = T1130514013 Laboratory ID = 20140860102 Lab Value = 0.069 Expected Conc. = 0.1002 Report level label = 0.01 Pct Recovery = 68% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 012513 Laboratory ID = 20133400002 Lab Value = 0.087 Expected Conc. = 0.1002 Report level label = 0.01 Pct Recovery = 87% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = 052412 Laboratory ID = 20132910008 Lab Value = 0.072 Expected Conc. = 0.1002 Report level label = 0.01 Pct Recovery = 72% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = 052412 Laboratory ID = 20131920149 Lab Value = 0.079 Expected Conc. = 0.1002 Report level label = 0.01 Pct Recovery = 79% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl SpecificMix = 012513 Laboratory ID = 20130650005 Lab Value = 0.067 Expected Conc. = 0.1002 Report level label = 0.01 Pct Recovery = 67% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl SpecificMix = 052412 Laboratory ID = 20131230084 Lab Value = 0.093 Expected Conc. = 0.0996 Report level label = 0.01 Pct Recovery = 93% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl SpecificMix = 05BB029 Laboratory ID = 20130510051 Lab Value = 0.061 Expected Conc. = 0.0996 Report level label = 0.01 Pct Recovery = 61% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl SpecificMix = 05BB029 Laboratory ID = 20140370077 Lab Value = 0.084 Expected Conc. = 0.095 Report level label = 0.01 Pct Recovery = 89% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl SpecificMix = T1130514013 Laboratory ID = 20132690010 Lab Value = 0.117 Expected Conc. = 0.095 Report level label = 0.01 Pct Recovery = 123% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl SpecificMix = T1130514013 Laboratory ID = 20131370001 Lab Value = 0.098 Expected Conc. = 0.095 Report level label = 0.01 Pct Recovery = 103% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl SpecificMix = 1473000 Laboratory ID = 20180390003 Lab Value = 0.051 Expected Conc. = 0.0663 Report level label = 0.01 Pct Recovery = 77% Analysis Date = 04/06/18 SpikeMix = Spex Organics EN170808006: 100 µl & Abs 071717Pest: 100 µl SpecificMix = EN170808006 Laboratory ID = 20163370001 Lab Value = 0.060 Expected Conc. = 0.0625 Report level label = 0.01 Pct Recovery = 96% Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl SpecificMix = LC20138V Laboratory ID = 20152610011 Lab Value = 0.045 Expected Conc. = 0.0601 Report level label = 0.01 Pct Recovery = 75% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl SpecificMix = 0406-15-01 Laboratory ID = 20152460215 Lab Value = 0.041 Expected Conc. = 0.0601 Report level label = 0.01 Pct Recovery = 69% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl SpecificMix = 0406-15-01 Laboratory ID = 20162860079 Lab Value = 0.055 Expected Conc. = 0.06 Report level label = 0.01 Pct Recovery = 91% Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl SpecificMix = 5054800 Laboratory ID = 20161880109 Lab Value = 0.080 Expected Conc. = 0.06 Report level label = 0.01 Pct Recovery = 133% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl SpecificMix = 5054800 Laboratory ID = 20171720140 Lab Value = 0.050 Expected Conc. = 0.05 Report level label = 0.01 Pct Recovery = 100% Analysis Date = 08/31/17 SpikeMix = Supelco LC20138V: 80 µl & Phenova B20160331: 80 µl SpecificMix = LC20138V Laboratory ID = 20170740063 Lab Value = 0.040 Expected Conc. = 0.05 Report level label = 0.01 Pct Recovery = 80% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl SpecificMix = LC20138V Laboratory ID = 20161470001 Lab Value = 0.051 Expected Conc. = 0.05 Report level label = 0.01 Pct Recovery = 101% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl SpecificMix = LC20138V Laboratory ID = 20171380001 Lab Value = 0.031 Expected Conc. = 0.048 Report level label = 0.01 Pct Recovery = 65% Analysis Date = 06/07/17 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 5054800 Laboratory ID = 20170960001 Lab Value = 0.047 Expected Conc. = 0.048 Report level label = 0.01 Pct Recovery = 98% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl SpecificMix = 5054800 Laboratory ID = 20161740258 Lab Value = 0.031 Expected Conc. = 0.048 Report level label = 0.01 Pct Recovery = 65% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 5054800 Laboratory ID = 20150720069 Lab Value = 0.035 Expected Conc. = 0.0402 Report level label = 0.01 Pct Recovery = 87% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 03DD006 Laboratory ID = 20143110108 Lab Value = 0.031 Expected Conc. = 0.0402 Report level label = 0.01 Pct Recovery = 78% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 03DD006 Laboratory ID = 20142960086 Lab Value = 0.029 Expected Conc. = 0.0402 Report level label = 0.01 Pct Recovery = 71% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 03DD006 Laboratory ID = 20142720002 Lab Value = 0.029 Expected Conc. = 0.0402 Report level label = 0.01 Pct Recovery = 72% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl SpecificMix = LC06435 Laboratory ID = 20142530087 Lab Value = 0.024 Expected Conc. = 0.0402 Report level label = 0.01 Pct Recovery = 60% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl SpecificMix = LC06435 Laboratory ID = 20142270001 Lab Value = 0.026 Expected Conc. = 0.0402 Report level label = 0.01 Pct Recovery = 64% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl SpecificMix = 03DD006 Laboratory ID = 20141570088 Lab Value = 0.036 Expected Conc. = 0.0402 Report level label = 0.01 Pct Recovery = 89% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl SpecificMix = LC06435 Laboratory ID = 20141220025 Lab Value = 0.041 Expected Conc. = 0.0402 Report level label = 0.01 Pct Recovery = 102% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl SpecificMix = LC06435 Laboratory ID = 20140730138 Lab Value = 0.033 Expected Conc. = 0.038 Report level label = 0.01 Pct Recovery = 86% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 1473000 Laboratory ID = 20133470008 Lab Value = 0.036 Expected Conc. = 0.038 Report level label = 0.01 Pct Recovery = 96% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl SpecificMix = 1473000 Laboratory ID = 20133310030 Lab Value = 0.033 Expected Conc. = 0.038 Report level label = 0.01 Pct Recovery = 86% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl SpecificMix = 1473000 Laboratory ID = 20133050050 Lab Value = 0.041 Expected Conc. = 0.038 Report level label = 0.01 Pct Recovery = 108% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl SpecificMix = T1130514013 Laboratory ID = 20132280016 Lab Value = 0.039 Expected Conc. = 0.038 Report level label = 0.01 Pct Recovery = 102% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl SpecificMix = T1130514013 Laboratory ID = 20131790009 Lab Value = 0.036 Expected Conc. = 0.038 Report level label = 0.01 Pct Recovery = 95% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl SpecificMix = 1473000 Laboratory ID = 20131650073 Lab Value = 0.036 Expected Conc. = 0.038 Report level label = 0.01 Pct Recovery = 95% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl SpecificMix = 1473000 Laboratory ID = 20172230001 Lab Value = 0.031 Expected Conc. = 0.035 Report level label = 0.01 Pct Recovery = 90% Analysis Date = 10/19/17 SpikeMix = ChemService 6472100: 50 µl & Abs 071717Pest: 50 µl SpecificMix = 6472100 Laboratory ID = 20181430122 Lab Value = 0.031 Expected Conc. = 0.0332 Report level label = 0.01 Pct Recovery = 94% Analysis Date = 06/20/18 SpikeMix = Abs 071817Pest: 50 µl & Spex Organics EN170808006: 50 µl SpecificMix = EN170808006 Laboratory ID = 20172560101 Lab Value = 0.028 Expected Conc. = 0.0332 Report level label = 0.01 Pct Recovery = 84% Analysis Date = 12/22/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6567600: 50 µl SpecificMix = EN170808006 Laboratory ID = 20172370001 Lab Value = 0.025 Expected Conc. = 0.0332 Report level label = 0.01 Pct Recovery = 77% Analysis Date = 11/18/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6537100: 50 µl SpecificMix = EN170808006 Laboratory ID = 20160770090 Lab Value = 0.019 Expected Conc. = 0.03 Report level label = 0.01 Pct Recovery = 64% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20160630046 Lab Value = 0.016 Expected Conc. = 0.03 Report level label = 0.01 Pct Recovery = 53% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20153510109 Lab Value = 0.020 Expected Conc. = 0.03 Report level label = 0.01 Pct Recovery = 67% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20153440001 Lab Value = 0.020 Expected Conc. = 0.03 Report level label = 0.01 Pct Recovery = 65% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20161260151 Lab Value = 0.021 Expected Conc. = 0.028 Report level label = 0.01 Pct Recovery = 75% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = 3851600 Laboratory ID = 20151550293 Lab Value = 0.027 Expected Conc. = 0.028 Report level label = 0.01 Pct Recovery = 96% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl SpecificMix = 3851600 Laboratory ID = 20151270112 Lab Value = 0.024 Expected Conc. = 0.028 Report level label = 0.01 Pct Recovery = 87% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl SpecificMix = 3851600 Laboratory ID = 20171510080 Lab Value = 0.025 Expected Conc. = 0.025 Report level label = 0.01 Pct Recovery = 98% Analysis Date = 06/09/17 SpikeMix = Supelco LC20138V: 40 µl & Crescent 03FF076: 40 µl SpecificMix = LC20138V Laboratory ID = 20162520001 Lab Value = 0.018 Expected Conc. = 0.025 Report level label = 0.01 Pct Recovery = 71% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl SpecificMix = LC20138V Laboratory ID = 20162660005 Lab Value = 0.020 Expected Conc. = 0.025 Report level label = 0.01 Pct Recovery = 79% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl SpecificMix = LC20138V Laboratory ID = 20162020124 Lab Value = 0.016 Expected Conc. = 0.025 Report level label = 0.01 Pct Recovery = 64% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl SpecificMix = LC20138V Laboratory ID = 20171940002 Lab Value = 0.018 Expected Conc. = 0.024 Report level label = 0.01 Pct Recovery = 76% Analysis Date = 11/10/17 SpikeMix = ChemService 5054800: 40 µl & NSI 041816: 40 µl SpecificMix = 5054800 Laboratory ID = 20170460061 Lab Value = 0.024 Expected Conc. = 0.024 Report level label = 0.01 Pct Recovery = 100% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl SpecificMix = 5054800 Laboratory ID = 20163560019 Lab Value = 0.019 Expected Conc. = 0.024 Report level label = 0.01 Pct Recovery = 79% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl SpecificMix = 5054800 Laboratory ID = 20162150213 Lab Value = 0.019 Expected Conc. = 0.024 Report level label = 0.01 Pct Recovery = 79% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl SpecificMix = 5054800 Laboratory ID = 20180940080 Lab Value = 0.016 Expected Conc. = 0.021 Report level label = 0.01 Pct Recovery = 76% Analysis Date = 05/31/18 SpikeMix = ChemService 6472100: 30 µl & Abs 071717Pest: 30 µl SpecificMix = 6472100 Laboratory ID = 20180050004 Lab Value = 0.018 Expected Conc. = 0.021 Report level label = 0.01 Pct Recovery = 83% Analysis Date = 04/05/18 SpikeMix = Abs 071817Pest: 30 µl & ChemService 6472100: 30 µl SpecificMix = 6472100 Laboratory ID = 20173120093 Lab Value = 0.018 Expected Conc. = 0.021 Report level label = 0.01 Pct Recovery = 87% Analysis Date = 03/10/18 SpikeMix = ChemService 6472100: 30 µl & ChemService 6537100: 30 µl SpecificMix = 6472100 Laboratory ID = 20150150115 Lab Value = 0.015 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 76% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl SpecificMix = LC06435 Laboratory ID = 20143370094 Lab Value = 0.010 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 48% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl SpecificMix = LC06435 Laboratory ID = 20142200164 Lab Value = 0.015 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 74% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 03DD006 Laboratory ID = 20141910243 Lab Value = 0.014 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 68% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = LC06435 Laboratory ID = 20141840097 Lab Value = 0.014 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 71% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl SpecificMix = LC06435 Laboratory ID = 20141640076 Lab Value = 0.018 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 89% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = 03DD006 Laboratory ID = 20141420140 Lab Value = 0.023 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 112% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 03DD006 Laboratory ID = 20141080004 Lab Value = 0.017 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 84% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl SpecificMix = 03DD006 Laboratory ID = 20152190003 Lab Value = 0.009 Expected Conc. = 0.015 Report level label = 0.01 Pct Recovery = 61% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = 0406-15-01 Laboratory ID = 20152040177 Lab Value = 0.012 Expected Conc. = 0.015 Report level label = 0.01 Pct Recovery = 78% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl SpecificMix = 0406-15-01 Laboratory ID = 20160430111 Lab Value = 0.012 Expected Conc. = 0.014 Report level label = 0.01 Pct Recovery = 84% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 3851600 Laboratory ID = 20160210080 Lab Value = 0.009 Expected Conc. = 0.014 Report level label = 0.01 Pct Recovery = 65% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 3851600 Laboratory ID = 20152950078 Lab Value = 0.008 Expected Conc. = 0.014 Report level label = 0.01 Pct Recovery = 60% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 3851600 Laboratory ID = 20153030068 Lab Value = 0.012 Expected Conc. = 0.014 Report level label = 0.01 Pct Recovery = 86% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = 3851600 Laboratory ID = 20151760208 Lab Value = 0.014 Expected Conc. = 0.014 Report level label = 0.01 Pct Recovery = 102% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl SpecificMix = 3851600 Laboratory ID = 20151380009 Lab Value = 0.011 Expected Conc. = 0.014 Report level label = 0.01 Pct Recovery = 79% Analysis Date = 05/30/15 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 3851600 Analysis Date = 06/20/18 Pct Recovery = 88% Analysis Date = 06/10/18 Pct Recovery = 87% Analysis Date = 06/10/18 Pct Recovery = 87% Analysis Date = 05/31/18 Pct Recovery = 87% Analysis Date = 05/31/18 Pct Recovery = 87% Analysis Date = 05/21/18 Pct Recovery = 87% Analysis Date = 05/21/18 Pct Recovery = 87% Analysis Date = 05/11/18 Pct Recovery = 87% Analysis Date = 05/11/18 Pct Recovery = 87% Analysis Date = 05/01/18 Pct Recovery = 87% Analysis Date = 05/01/18 Pct Recovery = 87% Analysis Date = 04/21/18 Pct Recovery = 87% Analysis Date = 04/21/18 Pct Recovery = 87% Analysis Date = 04/11/18 Pct Recovery = 87% Analysis Date = 04/11/18 Pct Recovery = 87% Analysis Date = 04/01/18 Pct Recovery = 87% Analysis Date = 04/01/18 Pct Recovery = 87% Analysis Date = 03/22/18 Pct Recovery = 87% Analysis Date = 03/22/18 Pct Recovery = 87% Analysis Date = 03/13/18 Pct Recovery = 87% Analysis Date = 03/13/18 Pct Recovery = 87% Analysis Date = 03/03/18 Pct Recovery = 86% Analysis Date = 03/03/18 Pct Recovery = 86% Analysis Date = 02/21/18 Pct Recovery = 86% Analysis Date = 02/21/18 Pct Recovery = 86% Analysis Date = 02/11/18 Pct Recovery = 86% Analysis Date = 02/11/18 Pct Recovery = 86% Analysis Date = 02/01/18 Pct Recovery = 86% Analysis Date = 02/01/18 Pct Recovery = 86% Analysis Date = 01/22/18 Pct Recovery = 86% Analysis Date = 01/22/18 Pct Recovery = 86% Analysis Date = 01/12/18 Pct Recovery = 86% Analysis Date = 01/12/18 Pct Recovery = 86% Analysis Date = 01/02/18 Pct Recovery = 86% Analysis Date = 01/02/18 Pct Recovery = 86% Analysis Date = 12/23/17 Pct Recovery = 86% Analysis Date = 12/23/17 Pct Recovery = 86% Analysis Date = 12/13/17 Pct Recovery = 86% Analysis Date = 12/13/17 Pct Recovery = 86% Analysis Date = 12/04/17 Pct Recovery = 86% Analysis Date = 12/04/17 Pct Recovery = 86% Analysis Date = 11/24/17 Pct Recovery = 85% Analysis Date = 11/24/17 Pct Recovery = 85% Analysis Date = 11/14/17 Pct Recovery = 85% Analysis Date = 11/14/17 Pct Recovery = 85% Analysis Date = 11/04/17 Pct Recovery = 85% Analysis Date = 11/04/17 Pct Recovery = 85% Analysis Date = 10/25/17 Pct Recovery = 85% Analysis Date = 10/25/17 Pct Recovery = 85% Analysis Date = 10/15/17 Pct Recovery = 85% Analysis Date = 10/15/17 Pct Recovery = 85% Analysis Date = 10/05/17 Pct Recovery = 85% Analysis Date = 10/05/17 Pct Recovery = 85% Analysis Date = 09/25/17 Pct Recovery = 85% Analysis Date = 09/25/17 Pct Recovery = 85% Analysis Date = 09/15/17 Pct Recovery = 85% Analysis Date = 09/15/17 Pct Recovery = 85% Analysis Date = 09/05/17 Pct Recovery = 84% Analysis Date = 09/05/17 Pct Recovery = 84% Analysis Date = 08/27/17 Pct Recovery = 84% Analysis Date = 08/27/17 Pct Recovery = 84% Analysis Date = 08/17/17 Pct Recovery = 84% Analysis Date = 08/17/17 Pct Recovery = 84% Analysis Date = 08/07/17 Pct Recovery = 84% Analysis Date = 08/07/17 Pct Recovery = 84% Analysis Date = 07/28/17 Pct Recovery = 84% Analysis Date = 07/28/17 Pct Recovery = 84% Analysis Date = 07/18/17 Pct Recovery = 84% Analysis Date = 07/18/17 Pct Recovery = 84% Analysis Date = 07/08/17 Pct Recovery = 84% Analysis Date = 07/08/17 Pct Recovery = 84% Analysis Date = 06/28/17 Pct Recovery = 84% Analysis Date = 06/28/17 Pct Recovery = 84% Analysis Date = 06/18/17 Pct Recovery = 84% Analysis Date = 06/18/17 Pct Recovery = 84% Analysis Date = 06/08/17 Pct Recovery = 83% Analysis Date = 06/08/17 Pct Recovery = 83% Analysis Date = 05/29/17 Pct Recovery = 83% Analysis Date = 05/29/17 Pct Recovery = 83% Analysis Date = 05/20/17 Pct Recovery = 83% Analysis Date = 05/20/17 Pct Recovery = 83% Analysis Date = 05/10/17 Pct Recovery = 83% Analysis Date = 05/10/17 Pct Recovery = 83% Analysis Date = 04/30/17 Pct Recovery = 83% Analysis Date = 04/30/17 Pct Recovery = 83% Analysis Date = 04/20/17 Pct Recovery = 83% Analysis Date = 04/20/17 Pct Recovery = 83% Analysis Date = 04/10/17 Pct Recovery = 83% Analysis Date = 04/10/17 Pct Recovery = 83% Analysis Date = 03/31/17 Pct Recovery = 83% Analysis Date = 03/31/17 Pct Recovery = 83% Analysis Date = 03/21/17 Pct Recovery = 83% Analysis Date = 03/21/17 Pct Recovery = 83% Analysis Date = 03/11/17 Pct Recovery = 82% Analysis Date = 03/11/17 Pct Recovery = 82% Analysis Date = 03/01/17 Pct Recovery = 82% Analysis Date = 03/01/17 Pct Recovery = 82% Analysis Date = 02/19/17 Pct Recovery = 82% Analysis Date = 02/19/17 Pct Recovery = 82% Analysis Date = 02/10/17 Pct Recovery = 82% Analysis Date = 02/10/17 Pct Recovery = 82% Analysis Date = 01/31/17 Pct Recovery = 82% Analysis Date = 01/31/17 Pct Recovery = 82% Analysis Date = 01/21/17 Pct Recovery = 82% Analysis Date = 01/21/17 Pct Recovery = 82% Analysis Date = 01/11/17 Pct Recovery = 82% Analysis Date = 01/11/17 Pct Recovery = 82% Analysis Date = 01/01/17 Pct Recovery = 82% Analysis Date = 01/01/17 Pct Recovery = 82% Analysis Date = 12/22/16 Pct Recovery = 82% Analysis Date = 12/22/16 Pct Recovery = 82% Analysis Date = 12/12/16 Pct Recovery = 82% Analysis Date = 12/12/16 Pct Recovery = 82% Analysis Date = 12/02/16 Pct Recovery = 81% Analysis Date = 12/02/16 Pct Recovery = 81% Analysis Date = 11/22/16 Pct Recovery = 81% Analysis Date = 11/22/16 Pct Recovery = 81% Analysis Date = 11/12/16 Pct Recovery = 81% Analysis Date = 11/12/16 Pct Recovery = 81% Analysis Date = 11/03/16 Pct Recovery = 81% Analysis Date = 11/03/16 Pct Recovery = 81% Analysis Date = 10/24/16 Pct Recovery = 81% Analysis Date = 10/24/16 Pct Recovery = 81% Analysis Date = 10/14/16 Pct Recovery = 81% Analysis Date = 10/14/16 Pct Recovery = 81% Analysis Date = 10/04/16 Pct Recovery = 81% Analysis Date = 10/04/16 Pct Recovery = 81% Analysis Date = 09/24/16 Pct Recovery = 81% Analysis Date = 09/24/16 Pct Recovery = 81% Analysis Date = 09/14/16 Pct Recovery = 81% Analysis Date = 09/14/16 Pct Recovery = 81% Analysis Date = 09/04/16 Pct Recovery = 80% Analysis Date = 09/04/16 Pct Recovery = 80% Analysis Date = 08/25/16 Pct Recovery = 80% Analysis Date = 08/25/16 Pct Recovery = 80% Analysis Date = 08/15/16 Pct Recovery = 80% Analysis Date = 08/15/16 Pct Recovery = 80% Analysis Date = 08/05/16 Pct Recovery = 80% Analysis Date = 08/05/16 Pct Recovery = 80% Analysis Date = 07/27/16 Pct Recovery = 80% Analysis Date = 07/27/16 Pct Recovery = 80% Analysis Date = 07/17/16 Pct Recovery = 80% Analysis Date = 07/17/16 Pct Recovery = 80% Analysis Date = 07/07/16 Pct Recovery = 80% Analysis Date = 07/07/16 Pct Recovery = 80% Analysis Date = 06/27/16 Pct Recovery = 80% Analysis Date = 06/27/16 Pct Recovery = 80% Analysis Date = 06/17/16 Pct Recovery = 80% Analysis Date = 06/17/16 Pct Recovery = 80% Analysis Date = 06/07/16 Pct Recovery = 79% Analysis Date = 06/07/16 Pct Recovery = 79% Analysis Date = 05/28/16 Pct Recovery = 79% Analysis Date = 05/28/16 Pct Recovery = 79% Analysis Date = 05/18/16 Pct Recovery = 79% Analysis Date = 05/18/16 Pct Recovery = 79% Analysis Date = 05/08/16 Pct Recovery = 79% Analysis Date = 05/08/16 Pct Recovery = 79% Analysis Date = 04/28/16 Pct Recovery = 79% Analysis Date = 04/28/16 Pct Recovery = 79% Analysis Date = 04/19/16 Pct Recovery = 79% Analysis Date = 04/19/16 Pct Recovery = 79% Analysis Date = 04/09/16 Pct Recovery = 79% Analysis Date = 04/09/16 Pct Recovery = 79% Analysis Date = 03/30/16 Pct Recovery = 78% Analysis Date = 03/30/16 Pct Recovery = 78% Analysis Date = 03/20/16 Pct Recovery = 78% Analysis Date = 03/20/16 Pct Recovery = 78% Analysis Date = 03/10/16 Pct Recovery = 78% Analysis Date = 03/10/16 Pct Recovery = 78% Analysis Date = 02/29/16 Pct Recovery = 78% Analysis Date = 02/29/16 Pct Recovery = 78% Analysis Date = 02/19/16 Pct Recovery = 78% Analysis Date = 02/19/16 Pct Recovery = 78% Analysis Date = 02/09/16 Pct Recovery = 78% Analysis Date = 02/09/16 Pct Recovery = 78% Analysis Date = 01/30/16 Pct Recovery = 78% Analysis Date = 01/30/16 Pct Recovery = 78% Analysis Date = 01/20/16 Pct Recovery = 77% Analysis Date = 01/20/16 Pct Recovery = 77% Analysis Date = 01/11/16 Pct Recovery = 77% Analysis Date = 01/11/16 Pct Recovery = 77% Analysis Date = 01/01/16 Pct Recovery = 77% Analysis Date = 01/01/16 Pct Recovery = 77% Analysis Date = 12/22/15 Pct Recovery = 77% Analysis Date = 12/22/15 Pct Recovery = 77% Analysis Date = 12/12/15 Pct Recovery = 77% Analysis Date = 12/12/15 Pct Recovery = 77% Analysis Date = 12/02/15 Pct Recovery = 77% Analysis Date = 12/02/15 Pct Recovery = 77% Analysis Date = 11/22/15 Pct Recovery = 77% Analysis Date = 11/22/15 Pct Recovery = 77% Analysis Date = 11/12/15 Pct Recovery = 77% Analysis Date = 11/12/15 Pct Recovery = 77% Analysis Date = 11/02/15 Pct Recovery = 76% Analysis Date = 11/02/15 Pct Recovery = 76% Analysis Date = 10/23/15 Pct Recovery = 76% Analysis Date = 10/23/15 Pct Recovery = 76% Analysis Date = 10/13/15 Pct Recovery = 76% Analysis Date = 10/13/15 Pct Recovery = 76% Analysis Date = 10/04/15 Pct Recovery = 76% Analysis Date = 10/04/15 Pct Recovery = 76% Analysis Date = 09/24/15 Pct Recovery = 76% Analysis Date = 09/24/15 Pct Recovery = 76% Analysis Date = 09/14/15 Pct Recovery = 76% Analysis Date = 09/14/15 Pct Recovery = 76% Analysis Date = 09/04/15 Pct Recovery = 76% Analysis Date = 09/04/15 Pct Recovery = 76% Analysis Date = 08/25/15 Pct Recovery = 76% Analysis Date = 08/25/15 Pct Recovery = 76% Analysis Date = 08/15/15 Pct Recovery = 76% Analysis Date = 08/15/15 Pct Recovery = 76% Analysis Date = 08/05/15 Pct Recovery = 76% Analysis Date = 08/05/15 Pct Recovery = 76% Analysis Date = 07/26/15 Pct Recovery = 76% Analysis Date = 07/26/15 Pct Recovery = 76% Analysis Date = 07/16/15 Pct Recovery = 76% Analysis Date = 07/16/15 Pct Recovery = 76% Analysis Date = 07/06/15 Pct Recovery = 76% Analysis Date = 07/06/15 Pct Recovery = 76% Analysis Date = 06/27/15 Pct Recovery = 76% Analysis Date = 06/27/15 Pct Recovery = 76% Analysis Date = 06/17/15 Pct Recovery = 76% Analysis Date = 06/17/15 Pct Recovery = 76% Analysis Date = 06/07/15 Pct Recovery = 76% Analysis Date = 06/07/15 Pct Recovery = 76% Analysis Date = 05/28/15 Pct Recovery = 76% Analysis Date = 05/28/15 Pct Recovery = 76% Analysis Date = 05/18/15 Pct Recovery = 76% Analysis Date = 05/18/15 Pct Recovery = 76% Analysis Date = 05/08/15 Pct Recovery = 76% Analysis Date = 05/08/15 Pct Recovery = 76% Analysis Date = 04/28/15 Pct Recovery = 76% Analysis Date = 04/28/15 Pct Recovery = 76% Analysis Date = 04/18/15 Pct Recovery = 76% Analysis Date = 04/18/15 Pct Recovery = 76% Analysis Date = 04/08/15 Pct Recovery = 77% Analysis Date = 04/08/15 Pct Recovery = 77% Analysis Date = 03/29/15 Pct Recovery = 77% Analysis Date = 03/29/15 Pct Recovery = 77% Analysis Date = 03/20/15 Pct Recovery = 77% Analysis Date = 03/20/15 Pct Recovery = 77% Analysis Date = 03/10/15 Pct Recovery = 77% Analysis Date = 03/10/15 Pct Recovery = 77% Analysis Date = 02/28/15 Pct Recovery = 77% Analysis Date = 02/28/15 Pct Recovery = 77% Analysis Date = 02/18/15 Pct Recovery = 78% Analysis Date = 02/18/15 Pct Recovery = 78% Analysis Date = 02/08/15 Pct Recovery = 78% Analysis Date = 02/08/15 Pct Recovery = 78% Analysis Date = 01/29/15 Pct Recovery = 78% Analysis Date = 01/29/15 Pct Recovery = 78% Analysis Date = 01/19/15 Pct Recovery = 78% Analysis Date = 01/19/15 Pct Recovery = 78% Analysis Date = 01/09/15 Pct Recovery = 78% Analysis Date = 01/09/15 Pct Recovery = 78% Analysis Date = 12/30/14 Pct Recovery = 79% Analysis Date = 12/30/14 Pct Recovery = 79% Analysis Date = 12/20/14 Pct Recovery = 79% Analysis Date = 12/20/14 Pct Recovery = 79% Analysis Date = 12/11/14 Pct Recovery = 79% Analysis Date = 12/11/14 Pct Recovery = 79% Analysis Date = 12/01/14 Pct Recovery = 79% Analysis Date = 12/01/14 Pct Recovery = 79% Analysis Date = 11/21/14 Pct Recovery = 79% Analysis Date = 11/21/14 Pct Recovery = 79% Analysis Date = 11/11/14 Pct Recovery = 80% Analysis Date = 11/11/14 Pct Recovery = 80% Analysis Date = 11/01/14 Pct Recovery = 80% Analysis Date = 11/01/14 Pct Recovery = 80% Analysis Date = 10/22/14 Pct Recovery = 80% Analysis Date = 10/22/14 Pct Recovery = 80% Analysis Date = 10/12/14 Pct Recovery = 80% Analysis Date = 10/12/14 Pct Recovery = 80% Analysis Date = 10/02/14 Pct Recovery = 81% Analysis Date = 10/02/14 Pct Recovery = 81% Analysis Date = 09/22/14 Pct Recovery = 81% Analysis Date = 09/22/14 Pct Recovery = 81% Analysis Date = 09/12/14 Pct Recovery = 81% Analysis Date = 09/12/14 Pct Recovery = 81% Analysis Date = 09/03/14 Pct Recovery = 81% Analysis Date = 09/03/14 Pct Recovery = 81% Analysis Date = 08/24/14 Pct Recovery = 81% Analysis Date = 08/24/14 Pct Recovery = 81% Analysis Date = 08/14/14 Pct Recovery = 82% Analysis Date = 08/14/14 Pct Recovery = 82% Analysis Date = 08/04/14 Pct Recovery = 82% Analysis Date = 08/04/14 Pct Recovery = 82% Analysis Date = 07/25/14 Pct Recovery = 82% Analysis Date = 07/25/14 Pct Recovery = 82% Analysis Date = 07/15/14 Pct Recovery = 82% Analysis Date = 07/15/14 Pct Recovery = 82% Analysis Date = 07/05/14 Pct Recovery = 83% Analysis Date = 07/05/14 Pct Recovery = 83% Analysis Date = 06/25/14 Pct Recovery = 83% Analysis Date = 06/25/14 Pct Recovery = 83% Analysis Date = 06/15/14 Pct Recovery = 83% Analysis Date = 06/15/14 Pct Recovery = 83% Analysis Date = 06/05/14 Pct Recovery = 83% Analysis Date = 06/05/14 Pct Recovery = 83% Analysis Date = 05/27/14 Pct Recovery = 84% Analysis Date = 05/27/14 Pct Recovery = 84% Analysis Date = 05/17/14 Pct Recovery = 84% Analysis Date = 05/17/14 Pct Recovery = 84% Analysis Date = 05/07/14 Pct Recovery = 84% Analysis Date = 05/07/14 Pct Recovery = 84% Analysis Date = 04/27/14 Pct Recovery = 84% Analysis Date = 04/27/14 Pct Recovery = 84% Analysis Date = 04/17/14 Pct Recovery = 84% Analysis Date = 04/17/14 Pct Recovery = 84% Analysis Date = 04/07/14 Pct Recovery = 85% Analysis Date = 04/07/14 Pct Recovery = 85% Analysis Date = 03/28/14 Pct Recovery = 85% Analysis Date = 03/28/14 Pct Recovery = 85% Analysis Date = 03/18/14 Pct Recovery = 85% Analysis Date = 03/18/14 Pct Recovery = 85% Analysis Date = 03/08/14 Pct Recovery = 85% Analysis Date = 03/08/14 Pct Recovery = 85% Analysis Date = 02/26/14 Pct Recovery = 85% Analysis Date = 02/26/14 Pct Recovery = 85% Analysis Date = 02/17/14 Pct Recovery = 86% Analysis Date = 02/17/14 Pct Recovery = 86% Analysis Date = 02/07/14 Pct Recovery = 86% Analysis Date = 02/07/14 Pct Recovery = 86% Analysis Date = 01/28/14 Pct Recovery = 86% Analysis Date = 01/28/14 Pct Recovery = 86% Analysis Date = 01/18/14 Pct Recovery = 86% Analysis Date = 01/18/14 Pct Recovery = 86% Analysis Date = 01/08/14 Pct Recovery = 86% Analysis Date = 01/08/14 Pct Recovery = 86% Analysis Date = 12/29/13 Pct Recovery = 86% Analysis Date = 12/29/13 Pct Recovery = 86% Analysis Date = 12/19/13 Pct Recovery = 87% Analysis Date = 12/19/13 Pct Recovery = 87% Analysis Date = 12/09/13 Pct Recovery = 87% Analysis Date = 12/09/13 Pct Recovery = 87% Analysis Date = 11/29/13 Pct Recovery = 87% Analysis Date = 11/29/13 Pct Recovery = 87% Analysis Date = 11/19/13 Pct Recovery = 87% Analysis Date = 11/19/13 Pct Recovery = 87% Analysis Date = 11/10/13 Pct Recovery = 87% Analysis Date = 11/10/13 Pct Recovery = 87% Analysis Date = 10/31/13 Pct Recovery = 88% Analysis Date = 10/31/13 Pct Recovery = 88% Analysis Date = 10/21/13 Pct Recovery = 88% Analysis Date = 10/21/13 Pct Recovery = 88% Analysis Date = 10/11/13 Pct Recovery = 88% Analysis Date = 10/11/13 Pct Recovery = 88% Analysis Date = 10/01/13 Pct Recovery = 88% Analysis Date = 10/01/13 Pct Recovery = 88% Analysis Date = 09/21/13 Pct Recovery = 88% Analysis Date = 09/21/13 Pct Recovery = 88% Analysis Date = 09/11/13 Pct Recovery = 89% Analysis Date = 09/11/13 Pct Recovery = 89% Analysis Date = 09/01/13 Pct Recovery = 89% Analysis Date = 09/01/13 Pct Recovery = 89% Analysis Date = 08/22/13 Pct Recovery = 89% Analysis Date = 08/22/13 Pct Recovery = 89% Analysis Date = 08/12/13 Pct Recovery = 89% Analysis Date = 08/12/13 Pct Recovery = 89% Analysis Date = 08/03/13 Pct Recovery = 89% Analysis Date = 08/03/13 Pct Recovery = 89% Analysis Date = 07/24/13 Pct Recovery = 89% Analysis Date = 07/24/13 Pct Recovery = 89% Analysis Date = 07/14/13 Pct Recovery = 90% Analysis Date = 07/14/13 Pct Recovery = 90% Analysis Date = 07/04/13 Pct Recovery = 90% Analysis Date = 07/04/13 Pct Recovery = 90% Analysis Date = 06/24/13 Pct Recovery = 90% Analysis Date = 06/24/13 Pct Recovery = 90% Analysis Date = 06/14/13 Pct Recovery = 90% Analysis Date = 06/14/13 Pct Recovery = 90% Analysis Date = 06/04/13 Pct Recovery = 90% Analysis Date = 06/04/13 Pct Recovery = 90% Analysis Date = 05/25/13 Pct Recovery = 91% Analysis Date = 05/25/13 Pct Recovery = 91% Analysis Date = 05/15/13 Pct Recovery = 91% Analysis Date = 05/15/13 Pct Recovery = 91% Analysis Date = 05/05/13 Pct Recovery = 91% Analysis Date = 05/05/13 Pct Recovery = 91% Analysis Date = 04/26/13 Pct Recovery = 91% Analysis Date = 04/26/13 Pct Recovery = 91% Analysis Date = 04/16/13 Pct Recovery = 91% Analysis Date = 04/16/13 Pct Recovery = 91% Analysis Date = 04/06/13 Pct Recovery = 91% Analysis Date = 04/06/13 Pct Recovery = 91% Analysis Date = 03/27/13 Pct Recovery = 92% Analysis Date = 03/27/13 Pct Recovery = 92% Analysis Date = 03/17/13 Pct Recovery = 92% Analysis Date = 03/17/13 Pct Recovery = 92% Analysis Date = 03/07/13 Pct Recovery = 92% Analysis Date = 03/07/13 Pct Recovery = 92% Analysis Date = 02/25/13 Pct Recovery = 92% Analysis Date = 02/25/13 Pct Recovery = 92% Analysis Date = 02/15/13 Pct Recovery = 92% Analysis Date = 02/15/13 Pct Recovery = 92% Analysis Date = 02/05/13 Pct Recovery = 92% Analysis Date = 02/05/13 Pct Recovery = 92% Analysis Date = 01/26/13 Pct Recovery = 93% Analysis Date = 01/26/13 Pct Recovery = 93% Analysis Date = 01/17/13 Pct Recovery = 93% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
CHLORPYRIFOS

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 82 83% 16% 82% 17%
Total 82 83% 16% 82% 17%

Sample Statistics
CHLORPYRIFOS

Characteristic N % % Basis
Plotted 82 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 82 .  
False Negatives 0 0% 0 out of 82
Not Spiked 52 .  
False Positives 0 0% 0 out of 52

OBSP Determination:
CHLORPYRIFOS, OXYGEN ANALOG
METHOD: 2033 , TESTIDCODE: 61636GCM39

Laboratory ID = 20140100085 Lab Value = 0.978 Expected Conc. = 1.5 Report level label = 0.08 Pct Recovery = 65% Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl SpecificMix = T1130514013 Laboratory ID = 20132490342 Lab Value = 0.204 Expected Conc. = 1.5 Report level label = 0.08 Pct Recovery = 14% Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl SpecificMix = T1130514013 Laboratory ID = 20140370077 Lab Value = 0.297 Expected Conc. = 0.75 Report level label = 0.08 Pct Recovery = 40% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl SpecificMix = T1130514013 Laboratory ID = 20132690010 Lab Value = 0.212 Expected Conc. = 0.75 Report level label = 0.08 Pct Recovery = 28% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl SpecificMix = T1130514013 Laboratory ID = 20131370001 Lab Value = 0.258 Expected Conc. = 0.75 Report level label = 0.08 Pct Recovery = 34% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl SpecificMix = 1473000 Laboratory ID = 20161880109 Lab Value = 0.246 Expected Conc. = 0.493 Report level label = 0.08 Pct Recovery = 50% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl SpecificMix = 03FF076 Laboratory ID = 20130250061 Lab Value = 0.152 Expected Conc. = 0.493 Report level label = 0.08 Pct Recovery = 31% Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl SpecificMix = 05BB029 Laboratory ID = 20152750006 Lab Value = 0.115 Expected Conc. = 0.4816 Report level label = 0.08 Pct Recovery = 24% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl SpecificMix = 040615 Laboratory ID = 20152610011 Lab Value = 0.196 Expected Conc. = 0.4816 Report level label = 0.08 Pct Recovery = 41% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl SpecificMix = 040615 Laboratory ID = 20170960001 Lab Value = 0.164 Expected Conc. = 0.3944 Report level label = 0.08 Pct Recovery = 42% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl SpecificMix = 03FF076 Laboratory ID = 20142720002 Lab Value = 0.094 Expected Conc. = 0.3198 Report level label = 0.08 Pct Recovery = 29% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl SpecificMix = LC06435 Laboratory ID = 20142530087 Lab Value = 0.059 Expected Conc. = 0.3198 Report level label = 0.08 Pct Recovery = 18% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl SpecificMix = LC06435 Laboratory ID = 20141570088 Lab Value = 0.121 Expected Conc. = 0.3198 Report level label = 0.08 Pct Recovery = 38% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl SpecificMix = LC06435 Laboratory ID = 20141220025 Lab Value = 0.189 Expected Conc. = 0.3198 Report level label = 0.08 Pct Recovery = 59% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl SpecificMix = LC06435 Laboratory ID = 20150720069 Lab Value = 0.125 Expected Conc. = 0.3168 Report level label = 0.08 Pct Recovery = 39% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 03DD006 Laboratory ID = 20143110108 Lab Value = 0.172 Expected Conc. = 0.3168 Report level label = 0.08 Pct Recovery = 54% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 03DD006 Laboratory ID = 20142960086 Lab Value = 0.102 Expected Conc. = 0.3168 Report level label = 0.08 Pct Recovery = 32% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 03DD006 Laboratory ID = 20142270001 Lab Value = 0.106 Expected Conc. = 0.3168 Report level label = 0.08 Pct Recovery = 33% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl SpecificMix = 03DD006 Laboratory ID = 20140730138 Lab Value = 0.121 Expected Conc. = 0.3 Report level label = 0.08 Pct Recovery = 40% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 1473000 Laboratory ID = 20133470008 Lab Value = 0.089 Expected Conc. = 0.3 Report level label = 0.08 Pct Recovery = 30% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl SpecificMix = 1473000 Laboratory ID = 20133310030 Lab Value = 0.202 Expected Conc. = 0.3 Report level label = 0.08 Pct Recovery = 67% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl SpecificMix = 1473000 Laboratory ID = 20133050050 Lab Value = 0.087 Expected Conc. = 0.3 Report level label = 0.08 Pct Recovery = 29% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl SpecificMix = T1130514013 Laboratory ID = 20132280016 Lab Value = 0.089 Expected Conc. = 0.3 Report level label = 0.08 Pct Recovery = 30% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl SpecificMix = T1130514013 Laboratory ID = 20131790009 Lab Value = 0.061 Expected Conc. = 0.3 Report level label = 0.08 Pct Recovery = 20% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl SpecificMix = 1473000 Laboratory ID = 20131650073 Lab Value = 0.064 Expected Conc. = 0.3 Report level label = 0.08 Pct Recovery = 21% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl SpecificMix = 1473000 Laboratory ID = 20172560101 Lab Value = 0.065 Expected Conc. = 0.271 Report level label = 0.08 Pct Recovery = 24% Analysis Date = 12/22/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6567600: 50 µl SpecificMix = EN170808006 Laboratory ID = 20172370001 Lab Value = 0.092 Expected Conc. = 0.271 Report level label = 0.08 Pct Recovery = 34% Analysis Date = 11/18/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6537100: 50 µl SpecificMix = EN170808006 Laboratory ID = 20172230001 Lab Value = 0.106 Expected Conc. = 0.265 Report level label = 0.08 Pct Recovery = 40% Analysis Date = 10/19/17 SpikeMix = ChemService 6472100: 50 µl & Abs 071717Pest: 50 µl SpecificMix = 6472100 Laboratory ID = 20140230082 Lab Value = 0.099 Expected Conc. = 0.2505 Report level label = 0.08 Pct Recovery = 40% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl SpecificMix = 012513 Laboratory ID = 20132420001 Lab Value = 0.112 Expected Conc. = 0.2505 Report level label = 0.08 Pct Recovery = 45% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl SpecificMix = 012513 Laboratory ID = 20151900132 Lab Value = 0.068 Expected Conc. = 0.2408 Report level label = 0.08 Pct Recovery = 28% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl SpecificMix = 040615 Laboratory ID = 20151550293 Lab Value = 0.055 Expected Conc. = 0.2408 Report level label = 0.08 Pct Recovery = 23% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl SpecificMix = 040615 Laboratory ID = 20161260151 Lab Value = 0.110 Expected Conc. = 0.24 Report level label = 0.08 Pct Recovery = 46% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = EN150513008 Laboratory ID = 20160770090 Lab Value = 0.109 Expected Conc. = 0.24 Report level label = 0.08 Pct Recovery = 45% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = EN150513008 Laboratory ID = 20153510109 Lab Value = 0.094 Expected Conc. = 0.24 Report level label = 0.08 Pct Recovery = 39% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = EN150513008 Laboratory ID = 20152330039 Lab Value = 0.071 Expected Conc. = 0.24 Report level label = 0.08 Pct Recovery = 30% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl SpecificMix = EN150513008 Laboratory ID = 20172020035 Lab Value = 0.104 Expected Conc. = 0.1972 Report level label = 0.08 Pct Recovery = 53% Analysis Date = 11/07/17 SpikeMix = Abs 071717Pest: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20171510080 Lab Value = 0.085 Expected Conc. = 0.1972 Report level label = 0.08 Pct Recovery = 43% Analysis Date = 06/09/17 SpikeMix = Supelco LC20138V: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20170460061 Lab Value = 0.067 Expected Conc. = 0.1972 Report level label = 0.08 Pct Recovery = 34% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl SpecificMix = 03FF076 Laboratory ID = 20162660005 Lab Value = 0.061 Expected Conc. = 0.1972 Report level label = 0.08 Pct Recovery = 31% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl SpecificMix = 03FF076 Laboratory ID = 20161600087 Lab Value = 0.124 Expected Conc. = 0.1972 Report level label = 0.08 Pct Recovery = 63% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20161340228 Lab Value = 0.107 Expected Conc. = 0.1972 Report level label = 0.08 Pct Recovery = 54% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl SpecificMix = 03FF076 Laboratory ID = 20161190075 Lab Value = 0.098 Expected Conc. = 0.1972 Report level label = 0.08 Pct Recovery = 50% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20150150115 Lab Value = 0.073 Expected Conc. = 0.1599 Report level label = 0.08 Pct Recovery = 46% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl SpecificMix = LC06435 Laboratory ID = 20143370094 Lab Value = 0.018 Expected Conc. = 0.1599 Report level label = 0.08 Pct Recovery = 11% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl SpecificMix = LC06435 Laboratory ID = 20141910243 Lab Value = 0.061 Expected Conc. = 0.1599 Report level label = 0.08 Pct Recovery = 38% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = LC06435 Laboratory ID = 20141840097 Lab Value = 0.040 Expected Conc. = 0.1599 Report level label = 0.08 Pct Recovery = 25% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl SpecificMix = LC06435 Laboratory ID = 20173120093 Lab Value = 0.066 Expected Conc. = 0.159 Report level label = 0.08 Pct Recovery = 42% Analysis Date = 03/10/18 SpikeMix = ChemService 6472100: 30 µl & ChemService 6537100: 30 µl SpecificMix = 6472100 Laboratory ID = 20142200164 Lab Value = 0.068 Expected Conc. = 0.1584 Report level label = 0.08 Pct Recovery = 43% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 03DD006 Laboratory ID = 20141640076 Lab Value = 0.070 Expected Conc. = 0.1584 Report level label = 0.08 Pct Recovery = 44% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = 03DD006 Laboratory ID = 20141420140 Lab Value = 0.057 Expected Conc. = 0.1584 Report level label = 0.08 Pct Recovery = 36% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 03DD006 Laboratory ID = 20141080004 Lab Value = 0.072 Expected Conc. = 0.1584 Report level label = 0.08 Pct Recovery = 45% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl SpecificMix = 03DD006 Laboratory ID = 20161050143 Lab Value = 0.076 Expected Conc. = 0.1204 Report level label = 0.08 Pct Recovery = 63% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Laboratory ID = 20160430111 Lab Value = 0.080 Expected Conc. = 0.1204 Report level label = 0.08 Pct Recovery = 66% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Laboratory ID = 20160070059 Lab Value = 0.070 Expected Conc. = 0.1204 Report level label = 0.08 Pct Recovery = 58% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = 040615 Laboratory ID = 20151380009 Lab Value = 0.031 Expected Conc. = 0.1204 Report level label = 0.08 Pct Recovery = 26% Analysis Date = 05/30/15 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Laboratory ID = 20151210037 Lab Value = 0.035 Expected Conc. = 0.1204 Report level label = 0.08 Pct Recovery = 29% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Laboratory ID = 20160560044 Lab Value = 0.067 Expected Conc. = 0.12 Report level label = 0.08 Pct Recovery = 56% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl SpecificMix = EN150513008 Laboratory ID = 20153030068 Lab Value = 0.033 Expected Conc. = 0.12 Report level label = 0.08 Pct Recovery = 28% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150513008 Laboratory ID = 20152190003 Lab Value = 0.024 Expected Conc. = 0.12 Report level label = 0.08 Pct Recovery = 20% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150513008 Laboratory ID = 20151480170 Lab Value = 0.051 Expected Conc. = 0.12 Report level label = 0.08 Pct Recovery = 43% Analysis Date = 06/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150513008 Laboratory ID = 20140860102 Lab Value = 0.021 Expected Conc. = 0.1002 Report level label = 0.08 Pct Recovery = 21% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 012513 Laboratory ID = 20131920149 Lab Value = 0.025 Expected Conc. = 0.1002 Report level label = 0.08 Pct Recovery = 25% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl SpecificMix = 012513 Laboratory ID = 20131230084 Lab Value = 0.075 Expected Conc. = 0.0986 Report level label = 0.08 Pct Recovery = 76% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl SpecificMix = 05BB029 Laboratory ID = 20130510051 Lab Value = 0.028 Expected Conc. = 0.0986 Report level label = 0.08 Pct Recovery = 28% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl SpecificMix = 05BB029 Analysis Date = 03/10/18 Pct Recovery = 40% Analysis Date = 02/28/18 Pct Recovery = 40% Analysis Date = 02/28/18 Pct Recovery = 40% Analysis Date = 02/19/18 Pct Recovery = 40% Analysis Date = 02/19/18 Pct Recovery = 40% Analysis Date = 02/10/18 Pct Recovery = 40% Analysis Date = 02/10/18 Pct Recovery = 40% Analysis Date = 01/31/18 Pct Recovery = 40% Analysis Date = 01/31/18 Pct Recovery = 40% Analysis Date = 01/22/18 Pct Recovery = 41% Analysis Date = 01/22/18 Pct Recovery = 41% Analysis Date = 01/13/18 Pct Recovery = 41% Analysis Date = 01/13/18 Pct Recovery = 41% Analysis Date = 01/03/18 Pct Recovery = 41% Analysis Date = 01/03/18 Pct Recovery = 41% Analysis Date = 12/25/17 Pct Recovery = 41% Analysis Date = 12/25/17 Pct Recovery = 41% Analysis Date = 12/16/17 Pct Recovery = 41% Analysis Date = 12/16/17 Pct Recovery = 41% Analysis Date = 12/07/17 Pct Recovery = 41% Analysis Date = 12/07/17 Pct Recovery = 41% Analysis Date = 11/27/17 Pct Recovery = 41% Analysis Date = 11/27/17 Pct Recovery = 41% Analysis Date = 11/18/17 Pct Recovery = 41% Analysis Date = 11/18/17 Pct Recovery = 41% Analysis Date = 11/09/17 Pct Recovery = 41% Analysis Date = 11/09/17 Pct Recovery = 41% Analysis Date = 10/30/17 Pct Recovery = 41% Analysis Date = 10/30/17 Pct Recovery = 41% Analysis Date = 10/21/17 Pct Recovery = 41% Analysis Date = 10/21/17 Pct Recovery = 41% Analysis Date = 10/12/17 Pct Recovery = 41% Analysis Date = 10/12/17 Pct Recovery = 41% Analysis Date = 10/03/17 Pct Recovery = 41% Analysis Date = 10/03/17 Pct Recovery = 41% Analysis Date = 09/23/17 Pct Recovery = 41% Analysis Date = 09/23/17 Pct Recovery = 41% Analysis Date = 09/14/17 Pct Recovery = 42% Analysis Date = 09/14/17 Pct Recovery = 42% Analysis Date = 09/05/17 Pct Recovery = 42% Analysis Date = 09/05/17 Pct Recovery = 42% Analysis Date = 08/26/17 Pct Recovery = 42% Analysis Date = 08/26/17 Pct Recovery = 42% Analysis Date = 08/17/17 Pct Recovery = 42% Analysis Date = 08/17/17 Pct Recovery = 42% Analysis Date = 08/08/17 Pct Recovery = 42% Analysis Date = 08/08/17 Pct Recovery = 42% Analysis Date = 07/30/17 Pct Recovery = 42% Analysis Date = 07/30/17 Pct Recovery = 42% Analysis Date = 07/20/17 Pct Recovery = 42% Analysis Date = 07/20/17 Pct Recovery = 42% Analysis Date = 07/11/17 Pct Recovery = 42% Analysis Date = 07/11/17 Pct Recovery = 42% Analysis Date = 07/02/17 Pct Recovery = 42% Analysis Date = 07/02/17 Pct Recovery = 42% Analysis Date = 06/22/17 Pct Recovery = 42% Analysis Date = 06/22/17 Pct Recovery = 42% Analysis Date = 06/13/17 Pct Recovery = 42% Analysis Date = 06/13/17 Pct Recovery = 42% Analysis Date = 06/04/17 Pct Recovery = 42% Analysis Date = 06/04/17 Pct Recovery = 42% Analysis Date = 05/26/17 Pct Recovery = 42% Analysis Date = 05/26/17 Pct Recovery = 42% Analysis Date = 05/16/17 Pct Recovery = 42% Analysis Date = 05/16/17 Pct Recovery = 42% Analysis Date = 05/07/17 Pct Recovery = 42% Analysis Date = 05/07/17 Pct Recovery = 42% Analysis Date = 04/28/17 Pct Recovery = 42% Analysis Date = 04/28/17 Pct Recovery = 42% Analysis Date = 04/18/17 Pct Recovery = 42% Analysis Date = 04/18/17 Pct Recovery = 42% Analysis Date = 04/09/17 Pct Recovery = 42% Analysis Date = 04/09/17 Pct Recovery = 42% Analysis Date = 03/31/17 Pct Recovery = 42% Analysis Date = 03/31/17 Pct Recovery = 42% Analysis Date = 03/21/17 Pct Recovery = 42% Analysis Date = 03/21/17 Pct Recovery = 42% Analysis Date = 03/12/17 Pct Recovery = 43% Analysis Date = 03/12/17 Pct Recovery = 43% Analysis Date = 03/03/17 Pct Recovery = 43% Analysis Date = 03/03/17 Pct Recovery = 43% Analysis Date = 02/22/17 Pct Recovery = 43% Analysis Date = 02/22/17 Pct Recovery = 43% Analysis Date = 02/12/17 Pct Recovery = 43% Analysis Date = 02/12/17 Pct Recovery = 43% Analysis Date = 02/03/17 Pct Recovery = 43% Analysis Date = 02/03/17 Pct Recovery = 43% Analysis Date = 01/25/17 Pct Recovery = 43% Analysis Date = 01/25/17 Pct Recovery = 43% Analysis Date = 01/15/17 Pct Recovery = 43% Analysis Date = 01/15/17 Pct Recovery = 43% Analysis Date = 01/06/17 Pct Recovery = 43% Analysis Date = 01/06/17 Pct Recovery = 43% Analysis Date = 12/28/16 Pct Recovery = 43% Analysis Date = 12/28/16 Pct Recovery = 43% Analysis Date = 12/19/16 Pct Recovery = 43% Analysis Date = 12/19/16 Pct Recovery = 43% Analysis Date = 12/09/16 Pct Recovery = 43% Analysis Date = 12/09/16 Pct Recovery = 43% Analysis Date = 11/30/16 Pct Recovery = 43% Analysis Date = 11/30/16 Pct Recovery = 43% Analysis Date = 11/21/16 Pct Recovery = 43% Analysis Date = 11/21/16 Pct Recovery = 43% Analysis Date = 11/11/16 Pct Recovery = 43% Analysis Date = 11/11/16 Pct Recovery = 43% Analysis Date = 11/02/16 Pct Recovery = 43% Analysis Date = 11/02/16 Pct Recovery = 43% Analysis Date = 10/24/16 Pct Recovery = 43% Analysis Date = 10/24/16 Pct Recovery = 43% Analysis Date = 10/15/16 Pct Recovery = 43% Analysis Date = 10/15/16 Pct Recovery = 43% Analysis Date = 10/05/16 Pct Recovery = 43% Analysis Date = 10/05/16 Pct Recovery = 43% Analysis Date = 09/26/16 Pct Recovery = 43% Analysis Date = 09/26/16 Pct Recovery = 43% Analysis Date = 09/17/16 Pct Recovery = 43% Analysis Date = 09/17/16 Pct Recovery = 43% Analysis Date = 09/07/16 Pct Recovery = 43% Analysis Date = 09/07/16 Pct Recovery = 43% Analysis Date = 08/29/16 Pct Recovery = 43% Analysis Date = 08/29/16 Pct Recovery = 43% Analysis Date = 08/20/16 Pct Recovery = 44% Analysis Date = 08/20/16 Pct Recovery = 44% Analysis Date = 08/11/16 Pct Recovery = 44% Analysis Date = 08/11/16 Pct Recovery = 44% Analysis Date = 08/01/16 Pct Recovery = 44% Analysis Date = 08/01/16 Pct Recovery = 44% Analysis Date = 07/23/16 Pct Recovery = 44% Analysis Date = 07/23/16 Pct Recovery = 44% Analysis Date = 07/14/16 Pct Recovery = 44% Analysis Date = 07/14/16 Pct Recovery = 44% Analysis Date = 07/04/16 Pct Recovery = 44% Analysis Date = 07/04/16 Pct Recovery = 44% Analysis Date = 06/25/16 Pct Recovery = 44% Analysis Date = 06/25/16 Pct Recovery = 44% Analysis Date = 06/16/16 Pct Recovery = 44% Analysis Date = 06/16/16 Pct Recovery = 44% Analysis Date = 06/06/16 Pct Recovery = 44% Analysis Date = 06/06/16 Pct Recovery = 44% Analysis Date = 05/28/16 Pct Recovery = 44% Analysis Date = 05/28/16 Pct Recovery = 44% Analysis Date = 05/19/16 Pct Recovery = 44% Analysis Date = 05/19/16 Pct Recovery = 44% Analysis Date = 05/10/16 Pct Recovery = 44% Analysis Date = 05/10/16 Pct Recovery = 44% Analysis Date = 04/30/16 Pct Recovery = 44% Analysis Date = 04/30/16 Pct Recovery = 44% Analysis Date = 04/21/16 Pct Recovery = 44% Analysis Date = 04/21/16 Pct Recovery = 44% Analysis Date = 04/12/16 Pct Recovery = 44% Analysis Date = 04/12/16 Pct Recovery = 44% Analysis Date = 04/02/16 Pct Recovery = 44% Analysis Date = 04/02/16 Pct Recovery = 44% Analysis Date = 03/24/16 Pct Recovery = 43% Analysis Date = 03/24/16 Pct Recovery = 43% Analysis Date = 03/15/16 Pct Recovery = 43% Analysis Date = 03/15/16 Pct Recovery = 43% Analysis Date = 03/06/16 Pct Recovery = 43% Analysis Date = 03/06/16 Pct Recovery = 43% Analysis Date = 02/25/16 Pct Recovery = 43% Analysis Date = 02/25/16 Pct Recovery = 43% Analysis Date = 02/16/16 Pct Recovery = 43% Analysis Date = 02/16/16 Pct Recovery = 43% Analysis Date = 02/07/16 Pct Recovery = 43% Analysis Date = 02/07/16 Pct Recovery = 43% Analysis Date = 01/28/16 Pct Recovery = 43% Analysis Date = 01/28/16 Pct Recovery = 43% Analysis Date = 01/19/16 Pct Recovery = 43% Analysis Date = 01/19/16 Pct Recovery = 43% Analysis Date = 01/10/16 Pct Recovery = 42% Analysis Date = 01/10/16 Pct Recovery = 42% Analysis Date = 01/01/16 Pct Recovery = 42% Analysis Date = 01/01/16 Pct Recovery = 42% Analysis Date = 12/22/15 Pct Recovery = 42% Analysis Date = 12/22/15 Pct Recovery = 42% Analysis Date = 12/13/15 Pct Recovery = 41% Analysis Date = 12/13/15 Pct Recovery = 41% Analysis Date = 12/04/15 Pct Recovery = 41% Analysis Date = 12/04/15 Pct Recovery = 41% Analysis Date = 11/24/15 Pct Recovery = 41% Analysis Date = 11/24/15 Pct Recovery = 41% Analysis Date = 11/15/15 Pct Recovery = 40% Analysis Date = 11/15/15 Pct Recovery = 40% Analysis Date = 11/06/15 Pct Recovery = 40% Analysis Date = 11/06/15 Pct Recovery = 40% Analysis Date = 10/28/15 Pct Recovery = 40% Analysis Date = 10/28/15 Pct Recovery = 40% Analysis Date = 10/18/15 Pct Recovery = 40% Analysis Date = 10/18/15 Pct Recovery = 40% Analysis Date = 10/09/15 Pct Recovery = 39% Analysis Date = 10/09/15 Pct Recovery = 39% Analysis Date = 09/30/15 Pct Recovery = 39% Analysis Date = 09/30/15 Pct Recovery = 39% Analysis Date = 09/20/15 Pct Recovery = 39% Analysis Date = 09/20/15 Pct Recovery = 39% Analysis Date = 09/11/15 Pct Recovery = 38% Analysis Date = 09/11/15 Pct Recovery = 38% Analysis Date = 09/02/15 Pct Recovery = 38% Analysis Date = 09/02/15 Pct Recovery = 38% Analysis Date = 08/24/15 Pct Recovery = 38% Analysis Date = 08/24/15 Pct Recovery = 38% Analysis Date = 08/14/15 Pct Recovery = 37% Analysis Date = 08/14/15 Pct Recovery = 37% Analysis Date = 08/05/15 Pct Recovery = 37% Analysis Date = 08/05/15 Pct Recovery = 37% Analysis Date = 07/27/15 Pct Recovery = 37% Analysis Date = 07/27/15 Pct Recovery = 37% Analysis Date = 07/17/15 Pct Recovery = 37% Analysis Date = 07/17/15 Pct Recovery = 37% Analysis Date = 07/08/15 Pct Recovery = 36% Analysis Date = 07/08/15 Pct Recovery = 36% Analysis Date = 06/29/15 Pct Recovery = 36% Analysis Date = 06/29/15 Pct Recovery = 36% Analysis Date = 06/19/15 Pct Recovery = 36% Analysis Date = 06/19/15 Pct Recovery = 36% Analysis Date = 06/10/15 Pct Recovery = 35% Analysis Date = 06/10/15 Pct Recovery = 35% Analysis Date = 06/01/15 Pct Recovery = 35% Analysis Date = 06/01/15 Pct Recovery = 35% Analysis Date = 05/23/15 Pct Recovery = 35% Analysis Date = 05/23/15 Pct Recovery = 35% Analysis Date = 05/13/15 Pct Recovery = 35% Analysis Date = 05/13/15 Pct Recovery = 35% Analysis Date = 05/04/15 Pct Recovery = 35% Analysis Date = 05/04/15 Pct Recovery = 35% Analysis Date = 04/25/15 Pct Recovery = 35% Analysis Date = 04/25/15 Pct Recovery = 35% Analysis Date = 04/15/15 Pct Recovery = 35% Analysis Date = 04/15/15 Pct Recovery = 35% Analysis Date = 04/06/15 Pct Recovery = 35% Analysis Date = 04/06/15 Pct Recovery = 35% Analysis Date = 03/28/15 Pct Recovery = 35% Analysis Date = 03/28/15 Pct Recovery = 35% Analysis Date = 03/19/15 Pct Recovery = 35% Analysis Date = 03/19/15 Pct Recovery = 35% Analysis Date = 03/09/15 Pct Recovery = 35% Analysis Date = 03/09/15 Pct Recovery = 35% Analysis Date = 02/28/15 Pct Recovery = 35% Analysis Date = 02/28/15 Pct Recovery = 35% Analysis Date = 02/19/15 Pct Recovery = 34% Analysis Date = 02/19/15 Pct Recovery = 34% Analysis Date = 02/09/15 Pct Recovery = 34% Analysis Date = 02/09/15 Pct Recovery = 34% Analysis Date = 01/31/15 Pct Recovery = 34% Analysis Date = 01/31/15 Pct Recovery = 34% Analysis Date = 01/22/15 Pct Recovery = 34% Analysis Date = 01/22/15 Pct Recovery = 34% Analysis Date = 01/13/15 Pct Recovery = 34% Analysis Date = 01/13/15 Pct Recovery = 34% Analysis Date = 01/03/15 Pct Recovery = 34% Analysis Date = 01/03/15 Pct Recovery = 34% Analysis Date = 12/25/14 Pct Recovery = 34% Analysis Date = 12/25/14 Pct Recovery = 34% Analysis Date = 12/16/14 Pct Recovery = 34% Analysis Date = 12/16/14 Pct Recovery = 34% Analysis Date = 12/06/14 Pct Recovery = 34% Analysis Date = 12/06/14 Pct Recovery = 34% Analysis Date = 11/27/14 Pct Recovery = 34% Analysis Date = 11/27/14 Pct Recovery = 34% Analysis Date = 11/18/14 Pct Recovery = 35% Analysis Date = 11/18/14 Pct Recovery = 35% Analysis Date = 11/09/14 Pct Recovery = 35% Analysis Date = 11/09/14 Pct Recovery = 35% Analysis Date = 10/30/14 Pct Recovery = 35% Analysis Date = 10/30/14 Pct Recovery = 35% Analysis Date = 10/21/14 Pct Recovery = 35% Analysis Date = 10/21/14 Pct Recovery = 35% Analysis Date = 10/12/14 Pct Recovery = 35% Analysis Date = 10/12/14 Pct Recovery = 35% Analysis Date = 10/02/14 Pct Recovery = 36% Analysis Date = 10/02/14 Pct Recovery = 36% Analysis Date = 09/23/14 Pct Recovery = 36% Analysis Date = 09/23/14 Pct Recovery = 36% Analysis Date = 09/14/14 Pct Recovery = 36% Analysis Date = 09/14/14 Pct Recovery = 36% Analysis Date = 09/04/14 Pct Recovery = 36% Analysis Date = 09/04/14 Pct Recovery = 36% Analysis Date = 08/26/14 Pct Recovery = 36% Analysis Date = 08/26/14 Pct Recovery = 36% Analysis Date = 08/17/14 Pct Recovery = 36% Analysis Date = 08/17/14 Pct Recovery = 36% Analysis Date = 08/08/14 Pct Recovery = 37% Analysis Date = 08/08/14 Pct Recovery = 37% Analysis Date = 07/29/14 Pct Recovery = 37% Analysis Date = 07/29/14 Pct Recovery = 37% Analysis Date = 07/20/14 Pct Recovery = 37% Analysis Date = 07/20/14 Pct Recovery = 37% Analysis Date = 07/11/14 Pct Recovery = 37% Analysis Date = 07/11/14 Pct Recovery = 37% Analysis Date = 07/01/14 Pct Recovery = 37% Analysis Date = 07/01/14 Pct Recovery = 37% Analysis Date = 06/22/14 Pct Recovery = 37% Analysis Date = 06/22/14 Pct Recovery = 37% Analysis Date = 06/13/14 Pct Recovery = 37% Analysis Date = 06/13/14 Pct Recovery = 37% Analysis Date = 06/04/14 Pct Recovery = 37% Analysis Date = 06/04/14 Pct Recovery = 37% Analysis Date = 05/25/14 Pct Recovery = 37% Analysis Date = 05/25/14 Pct Recovery = 37% Analysis Date = 05/16/14 Pct Recovery = 37% Analysis Date = 05/16/14 Pct Recovery = 37% Analysis Date = 05/07/14 Pct Recovery = 37% Analysis Date = 05/07/14 Pct Recovery = 37% Analysis Date = 04/27/14 Pct Recovery = 37% Analysis Date = 04/27/14 Pct Recovery = 37% Analysis Date = 04/18/14 Pct Recovery = 37% Analysis Date = 04/18/14 Pct Recovery = 37% Analysis Date = 04/09/14 Pct Recovery = 37% Analysis Date = 04/09/14 Pct Recovery = 37% Analysis Date = 03/31/14 Pct Recovery = 37% Analysis Date = 03/31/14 Pct Recovery = 37% Analysis Date = 03/21/14 Pct Recovery = 37% Analysis Date = 03/21/14 Pct Recovery = 37% Analysis Date = 03/12/14 Pct Recovery = 37% Analysis Date = 03/12/14 Pct Recovery = 37% Analysis Date = 03/03/14 Pct Recovery = 37% Analysis Date = 03/03/14 Pct Recovery = 37% Analysis Date = 02/21/14 Pct Recovery = 37% Analysis Date = 02/21/14 Pct Recovery = 37% Analysis Date = 02/12/14 Pct Recovery = 37% Analysis Date = 02/12/14 Pct Recovery = 37% Analysis Date = 02/03/14 Pct Recovery = 37% Analysis Date = 02/03/14 Pct Recovery = 37% Analysis Date = 01/25/14 Pct Recovery = 37% Analysis Date = 01/25/14 Pct Recovery = 37% Analysis Date = 01/15/14 Pct Recovery = 37% Analysis Date = 01/15/14 Pct Recovery = 37% Analysis Date = 01/06/14 Pct Recovery = 37% Analysis Date = 01/06/14 Pct Recovery = 37% Analysis Date = 12/28/13 Pct Recovery = 37% Analysis Date = 12/28/13 Pct Recovery = 37% Analysis Date = 12/18/13 Pct Recovery = 37% Analysis Date = 12/18/13 Pct Recovery = 37% Analysis Date = 12/09/13 Pct Recovery = 37% Analysis Date = 12/09/13 Pct Recovery = 37% Analysis Date = 11/30/13 Pct Recovery = 37% Analysis Date = 11/30/13 Pct Recovery = 37% Analysis Date = 11/20/13 Pct Recovery = 36% Analysis Date = 11/20/13 Pct Recovery = 36% Analysis Date = 11/11/13 Pct Recovery = 36% Analysis Date = 11/11/13 Pct Recovery = 36% Analysis Date = 11/02/13 Pct Recovery = 36% Analysis Date = 11/02/13 Pct Recovery = 36% Analysis Date = 10/24/13 Pct Recovery = 36% Analysis Date = 10/24/13 Pct Recovery = 36% Analysis Date = 10/14/13 Pct Recovery = 36% Analysis Date = 10/14/13 Pct Recovery = 36% Analysis Date = 10/05/13 Pct Recovery = 36% Analysis Date = 10/05/13 Pct Recovery = 36% Analysis Date = 09/26/13 Pct Recovery = 36% Analysis Date = 09/26/13 Pct Recovery = 36% Analysis Date = 09/16/13 Pct Recovery = 36% Analysis Date = 09/16/13 Pct Recovery = 36% Analysis Date = 09/07/13 Pct Recovery = 36% Analysis Date = 09/07/13 Pct Recovery = 36% Analysis Date = 08/29/13 Pct Recovery = 36% Analysis Date = 08/29/13 Pct Recovery = 36% Analysis Date = 08/20/13 Pct Recovery = 36% Analysis Date = 08/20/13 Pct Recovery = 36% Analysis Date = 08/10/13 Pct Recovery = 36% Analysis Date = 08/10/13 Pct Recovery = 36% Analysis Date = 08/01/13 Pct Recovery = 36% Analysis Date = 08/01/13 Pct Recovery = 36% Analysis Date = 07/23/13 Pct Recovery = 36% Analysis Date = 07/23/13 Pct Recovery = 36% Analysis Date = 07/13/13 Pct Recovery = 36% Analysis Date = 07/13/13 Pct Recovery = 36% Analysis Date = 07/04/13 Pct Recovery = 35% Analysis Date = 07/04/13 Pct Recovery = 35% Analysis Date = 06/25/13 Pct Recovery = 35% Analysis Date = 06/25/13 Pct Recovery = 35% Analysis Date = 06/16/13 Pct Recovery = 35% Analysis Date = 06/16/13 Pct Recovery = 35% Analysis Date = 06/06/13 Pct Recovery = 35% Analysis Date = 06/06/13 Pct Recovery = 35% Analysis Date = 05/28/13 Pct Recovery = 35% Analysis Date = 05/28/13 Pct Recovery = 35% Analysis Date = 05/19/13 Pct Recovery = 35% Analysis Date = 05/19/13 Pct Recovery = 35% Analysis Date = 05/09/13 Pct Recovery = 35% Analysis Date = 05/09/13 Pct Recovery = 35% Analysis Date = 04/30/13 Pct Recovery = 35% Analysis Date = 04/30/13 Pct Recovery = 35% Analysis Date = 04/21/13 Pct Recovery = 35% Analysis Date = 04/21/13 Pct Recovery = 35% Analysis Date = 04/12/13 Pct Recovery = 35% Analysis Date = 04/12/13 Pct Recovery = 35% Analysis Date = 04/02/13 Pct Recovery = 34% Analysis Date = 04/02/13 Pct Recovery = 34% Analysis Date = 03/24/13 Pct Recovery = 34% Analysis Date = 03/24/13 Pct Recovery = 34% Analysis Date = 03/15/13 Pct Recovery = 34% Analysis Date = 03/15/13 Pct Recovery = 34% Analysis Date = 03/05/13 Pct Recovery = 34% Analysis Date = 03/05/13 Pct Recovery = 34% Analysis Date = 02/24/13 Pct Recovery = 34% Analysis Date = 02/24/13 Pct Recovery = 34% Analysis Date = 02/15/13 Pct Recovery = 34% Analysis Date = 02/15/13 Pct Recovery = 34% Analysis Date = 02/06/13 Pct Recovery = 34% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
CHLORPYRIFOS, OXYGEN ANALOG

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 65 38% 14% 38% 13%
Total 65 38% 14% 38% 13%

Sample Statistics
CHLORPYRIFOS, OXYGEN ANALOG

Characteristic N % % Basis
Plotted 65 98% Spiked
Estimated Values 65 98% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 66 .  
False Negatives 1 2% 1 out of 66
Not Spiked 47 .  
False Positives 0 0% 0 out of 47

OBSP Determination:
CIS-PERMETHRIN
METHOD: 2033 , TESTIDCODE: 82687GCM35

Laboratory ID = 20132490342 Lab Value = 0.058 Expected Conc. = 0.1 Report level label = 0.01 Pct Recovery = 58% Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20180390003 Lab Value = 0.030 Expected Conc. = 0.0669 Report level label = 0.012 Pct Recovery = 45% Analysis Date = 04/06/18 SpikeMix = Spex Organics EN170808006: 100 µl & Abs 071717Pest: 100 µl SpecificMix = EN170808006 Laboratory ID = 20163370001 Lab Value = 0.023 Expected Conc. = 0.0628 Report level label = 0.01 Pct Recovery = 37% Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl SpecificMix = B20160331 Laboratory ID = 20163150006 Lab Value = 0.021 Expected Conc. = 0.0628 Report level label = 0.01 Pct Recovery = 33% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl SpecificMix = B20160331 Laboratory ID = 20161880109 Lab Value = 0.071 Expected Conc. = 0.062 Report level label = 0.01 Pct Recovery = 115% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl SpecificMix = 03FF076 Laboratory ID = 20152610011 Lab Value = 0.038 Expected Conc. = 0.0598 Report level label = 0.01 Pct Recovery = 63% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl SpecificMix = 0406-15-01 Laboratory ID = 20152460215 Lab Value = 0.033 Expected Conc. = 0.0598 Report level label = 0.01 Pct Recovery = 56% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl SpecificMix = 0406-15-01 Laboratory ID = 20130940097 Lab Value = 0.031 Expected Conc. = 0.051 Report level label = 0.01 Pct Recovery = 60% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = 0507-12-04.2 Laboratory ID = 20123560092 Lab Value = 0.019 Expected Conc. = 0.051 Report level label = 0.01 Pct Recovery = 37% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = 0507-12-04.2 Laboratory ID = 20171720140 Lab Value = 0.021 Expected Conc. = 0.0502 Report level label = 0.01 Pct Recovery = 42% Analysis Date = 08/31/17 SpikeMix = Supelco LC20138V: 80 µl & Phenova B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20171660002 Lab Value = 0.018 Expected Conc. = 0.0502 Report level label = 0.01 Pct Recovery = 35% Analysis Date = 08/23/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20170190026 Lab Value = 0.013 Expected Conc. = 0.0502 Report level label = 0.01 Pct Recovery = 26% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20161470001 Lab Value = 0.025 Expected Conc. = 0.0502 Report level label = 0.01 Pct Recovery = 51% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20140370077 Lab Value = 0.023 Expected Conc. = 0.05 Report level label = 0.01 Pct Recovery = 46% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20132560001 Lab Value = 0.027 Expected Conc. = 0.05 Report level label = 0.01 Pct Recovery = 54% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20132140002 Lab Value = 0.027 Expected Conc. = 0.05 Report level label = 0.01 Pct Recovery = 55% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl SpecificMix = LB99392 Laboratory ID = 20131370001 Lab Value = 0.048 Expected Conc. = 0.05 Report level label = 0.01 Pct Recovery = 95% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl SpecificMix = LB99392 Laboratory ID = 20130810108 Lab Value = 0.036 Expected Conc. = 0.05 Report level label = 0.01 Pct Recovery = 72% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl SpecificMix = LB92783 Laboratory ID = 20130100066 Lab Value = 0.035 Expected Conc. = 0.05 Report level label = 0.01 Pct Recovery = 69% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl SpecificMix = LB92783 Laboratory ID = 20170960001 Lab Value = 0.033 Expected Conc. = 0.0496 Report level label = 0.01 Pct Recovery = 66% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl SpecificMix = 03FF076 Laboratory ID = 20143240095 Lab Value = 0.030 Expected Conc. = 0.0402 Report level label = 0.01 Pct Recovery = 73% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl SpecificMix = 032714 Laboratory ID = 20142270001 Lab Value = 0.019 Expected Conc. = 0.0402 Report level label = 0.01 Pct Recovery = 48% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl SpecificMix = 032714 Laboratory ID = 20141220025 Lab Value = 0.027 Expected Conc. = 0.0402 Report level label = 0.01 Pct Recovery = 67% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl SpecificMix = 032714 Laboratory ID = 20150430092 Lab Value = 0.030 Expected Conc. = 0.0401 Report level label = 0.01 Pct Recovery = 74% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl SpecificMix = E1140407002 Laboratory ID = 20143110108 Lab Value = 0.022 Expected Conc. = 0.0401 Report level label = 0.01 Pct Recovery = 56% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl SpecificMix = E1140407002 Laboratory ID = 20142720002 Lab Value = 0.021 Expected Conc. = 0.0401 Report level label = 0.01 Pct Recovery = 53% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl SpecificMix = E1140407002 Laboratory ID = 20141770149 Lab Value = 0.019 Expected Conc. = 0.0401 Report level label = 0.01 Pct Recovery = 48% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl SpecificMix = E1140407002 Laboratory ID = 20181430122 Lab Value = 0.027 Expected Conc. = 0.0335 Report level label = 0.012 Pct Recovery = 81% Analysis Date = 06/20/18 SpikeMix = Abs 071817Pest: 50 µl & Spex Organics EN170808006: 50 µl SpecificMix = EN170808006 Laboratory ID = 20172560101 Lab Value = 0.031 Expected Conc. = 0.0335 Report level label = 0.01 Pct Recovery = 93% Analysis Date = 12/22/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6567600: 50 µl SpecificMix = EN170808006 Laboratory ID = 20172370001 Lab Value = 0.038 Expected Conc. = 0.0335 Report level label = 0.01 Pct Recovery = 113% Analysis Date = 11/18/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6537100: 50 µl SpecificMix = EN170808006 Laboratory ID = 20161260151 Lab Value = 0.022 Expected Conc. = 0.032 Report level label = 0.01 Pct Recovery = 68% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = 3851600 Laboratory ID = 20151550293 Lab Value = 0.024 Expected Conc. = 0.032 Report level label = 0.01 Pct Recovery = 76% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl SpecificMix = 3851600 Laboratory ID = 20151270112 Lab Value = 0.024 Expected Conc. = 0.032 Report level label = 0.01 Pct Recovery = 73% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl SpecificMix = 3851600 Laboratory ID = 20160770090 Lab Value = 0.021 Expected Conc. = 0.0299 Report level label = 0.01 Pct Recovery = 71% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20160630046 Lab Value = 0.020 Expected Conc. = 0.0299 Report level label = 0.01 Pct Recovery = 66% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20153510109 Lab Value = 0.015 Expected Conc. = 0.0299 Report level label = 0.01 Pct Recovery = 49% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20153440001 Lab Value = 0.016 Expected Conc. = 0.0299 Report level label = 0.01 Pct Recovery = 54% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20171160110 Lab Value = 0.009 Expected Conc. = 0.0251 Report level label = 0.01 Pct Recovery = 36% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = B20160331 Laboratory ID = 20162380004 Lab Value = 0.011 Expected Conc. = 0.0251 Report level label = 0.01 Pct Recovery = 42% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = B20160331 Laboratory ID = 20162150213 Lab Value = 0.010 Expected Conc. = 0.0251 Report level label = 0.01 Pct Recovery = 38% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl SpecificMix = B20160331 Laboratory ID = 20172020035 Lab Value = 0.027 Expected Conc. = 0.0248 Report level label = 0.01 Pct Recovery = 107% Analysis Date = 11/07/17 SpikeMix = Abs 071717Pest: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20171510080 Lab Value = 0.023 Expected Conc. = 0.0248 Report level label = 0.01 Pct Recovery = 92% Analysis Date = 06/09/17 SpikeMix = Supelco LC20138V: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20170460061 Lab Value = 0.017 Expected Conc. = 0.0248 Report level label = 0.01 Pct Recovery = 68% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl SpecificMix = 03FF076 Laboratory ID = 20162660005 Lab Value = 0.022 Expected Conc. = 0.0248 Report level label = 0.01 Pct Recovery = 90% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl SpecificMix = 03FF076 Laboratory ID = 20161600087 Lab Value = 0.021 Expected Conc. = 0.0248 Report level label = 0.01 Pct Recovery = 84% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20161340228 Lab Value = 0.020 Expected Conc. = 0.0248 Report level label = 0.01 Pct Recovery = 81% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl SpecificMix = 03FF076 Laboratory ID = 20161190075 Lab Value = 0.019 Expected Conc. = 0.0248 Report level label = 0.01 Pct Recovery = 78% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20130510051 Lab Value = 0.011 Expected Conc. = 0.0204 Report level label = 0.01 Pct Recovery = 54% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl SpecificMix = 0507-12-04.2 Laboratory ID = 20150150115 Lab Value = 0.016 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 79% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl SpecificMix = 032714 Laboratory ID = 20142820151 Lab Value = 0.018 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 90% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl SpecificMix = 032714 Laboratory ID = 20141490205 Lab Value = 0.014 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 70% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = 032714 Laboratory ID = 20141080004 Lab Value = 0.011 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 56% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl SpecificMix = 032714 Laboratory ID = 20142470041 Lab Value = 0.012 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 61% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141910243 Lab Value = 0.010 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 51% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141640076 Lab Value = 0.013 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 63% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141360094 Lab Value = 0.010 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 49% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = E1140407002 Laboratory ID = 20140510043 Lab Value = 0.014 Expected Conc. = 0.02 Report level label = 0.01 Pct Recovery = 68% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl SpecificMix = LB99392 Laboratory ID = 20133580036 Lab Value = 0.008 Expected Conc. = 0.02 Report level label = 0.01 Pct Recovery = 40% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20133470008 Lab Value = 0.011 Expected Conc. = 0.02 Report level label = 0.01 Pct Recovery = 53% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl SpecificMix = LB99392 Laboratory ID = 20133190012 Lab Value = 0.019 Expected Conc. = 0.02 Report level label = 0.01 Pct Recovery = 93% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = LB99392 Laboratory ID = 20133050050 Lab Value = 0.017 Expected Conc. = 0.02 Report level label = 0.01 Pct Recovery = 86% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl SpecificMix = LB99392 Laboratory ID = 20131790009 Lab Value = 0.010 Expected Conc. = 0.02 Report level label = 0.01 Pct Recovery = 49% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20131510026 Lab Value = 0.017 Expected Conc. = 0.02 Report level label = 0.01 Pct Recovery = 85% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20130390105 Lab Value = 0.010 Expected Conc. = 0.02 Report level label = 0.01 Pct Recovery = 50% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl SpecificMix = LB92783 Laboratory ID = 20160430111 Lab Value = 0.013 Expected Conc. = 0.016 Report level label = 0.01 Pct Recovery = 81% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 3851600 Laboratory ID = 20160210080 Lab Value = 0.011 Expected Conc. = 0.016 Report level label = 0.01 Pct Recovery = 66% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 3851600 Laboratory ID = 20152950078 Lab Value = 0.009 Expected Conc. = 0.016 Report level label = 0.01 Pct Recovery = 54% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 3851600 Laboratory ID = 20153030068 Lab Value = 0.011 Expected Conc. = 0.016 Report level label = 0.01 Pct Recovery = 67% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = 3851600 Laboratory ID = 20151760208 Lab Value = 0.022 Expected Conc. = 0.016 Report level label = 0.01 Pct Recovery = 139% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl SpecificMix = 3851600 Laboratory ID = 20151380009 Lab Value = 0.007 Expected Conc. = 0.016 Report level label = 0.01 Pct Recovery = 44% Analysis Date = 05/30/15 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 3851600 Laboratory ID = 20152190003 Lab Value = 0.009 Expected Conc. = 0.0149 Report level label = 0.01 Pct Recovery = 62% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = 0406-15-01 Laboratory ID = 20152040177 Lab Value = 0.013 Expected Conc. = 0.0149 Report level label = 0.01 Pct Recovery = 90% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl SpecificMix = 0406-15-01 Analysis Date = 06/19/18 Pct Recovery = 70% Analysis Date = 06/10/18 Pct Recovery = 70% Analysis Date = 06/10/18 Pct Recovery = 70% Analysis Date = 05/31/18 Pct Recovery = 70% Analysis Date = 05/31/18 Pct Recovery = 70% Analysis Date = 05/21/18 Pct Recovery = 70% Analysis Date = 05/21/18 Pct Recovery = 70% Analysis Date = 05/11/18 Pct Recovery = 69% Analysis Date = 05/11/18 Pct Recovery = 69% Analysis Date = 05/01/18 Pct Recovery = 69% Analysis Date = 05/01/18 Pct Recovery = 69% Analysis Date = 04/21/18 Pct Recovery = 69% Analysis Date = 04/21/18 Pct Recovery = 69% Analysis Date = 04/11/18 Pct Recovery = 69% Analysis Date = 04/11/18 Pct Recovery = 69% Analysis Date = 04/01/18 Pct Recovery = 69% Analysis Date = 04/01/18 Pct Recovery = 69% Analysis Date = 03/22/18 Pct Recovery = 69% Analysis Date = 03/22/18 Pct Recovery = 69% Analysis Date = 03/12/18 Pct Recovery = 69% Analysis Date = 03/12/18 Pct Recovery = 69% Analysis Date = 03/02/18 Pct Recovery = 69% Analysis Date = 03/02/18 Pct Recovery = 69% Analysis Date = 02/21/18 Pct Recovery = 69% Analysis Date = 02/21/18 Pct Recovery = 69% Analysis Date = 02/11/18 Pct Recovery = 68% Analysis Date = 02/11/18 Pct Recovery = 68% Analysis Date = 02/01/18 Pct Recovery = 68% Analysis Date = 02/01/18 Pct Recovery = 68% Analysis Date = 01/22/18 Pct Recovery = 68% Analysis Date = 01/22/18 Pct Recovery = 68% Analysis Date = 01/12/18 Pct Recovery = 68% Analysis Date = 01/12/18 Pct Recovery = 68% Analysis Date = 01/02/18 Pct Recovery = 68% Analysis Date = 01/02/18 Pct Recovery = 68% Analysis Date = 12/23/17 Pct Recovery = 68% Analysis Date = 12/23/17 Pct Recovery = 68% Analysis Date = 12/13/17 Pct Recovery = 68% Analysis Date = 12/13/17 Pct Recovery = 68% Analysis Date = 12/03/17 Pct Recovery = 68% Analysis Date = 12/03/17 Pct Recovery = 68% Analysis Date = 11/23/17 Pct Recovery = 68% Analysis Date = 11/23/17 Pct Recovery = 68% Analysis Date = 11/13/17 Pct Recovery = 67% Analysis Date = 11/13/17 Pct Recovery = 67% Analysis Date = 11/04/17 Pct Recovery = 67% Analysis Date = 11/04/17 Pct Recovery = 67% Analysis Date = 10/25/17 Pct Recovery = 67% Analysis Date = 10/25/17 Pct Recovery = 67% Analysis Date = 10/15/17 Pct Recovery = 67% Analysis Date = 10/15/17 Pct Recovery = 67% Analysis Date = 10/05/17 Pct Recovery = 67% Analysis Date = 10/05/17 Pct Recovery = 67% Analysis Date = 09/25/17 Pct Recovery = 67% Analysis Date = 09/25/17 Pct Recovery = 67% Analysis Date = 09/15/17 Pct Recovery = 67% Analysis Date = 09/15/17 Pct Recovery = 67% Analysis Date = 09/05/17 Pct Recovery = 67% Analysis Date = 09/05/17 Pct Recovery = 67% Analysis Date = 08/26/17 Pct Recovery = 67% Analysis Date = 08/26/17 Pct Recovery = 67% Analysis Date = 08/16/17 Pct Recovery = 67% Analysis Date = 08/16/17 Pct Recovery = 67% Analysis Date = 08/06/17 Pct Recovery = 67% Analysis Date = 08/06/17 Pct Recovery = 67% Analysis Date = 07/27/17 Pct Recovery = 67% Analysis Date = 07/27/17 Pct Recovery = 67% Analysis Date = 07/18/17 Pct Recovery = 67% Analysis Date = 07/18/17 Pct Recovery = 67% Analysis Date = 07/08/17 Pct Recovery = 67% Analysis Date = 07/08/17 Pct Recovery = 67% Analysis Date = 06/28/17 Pct Recovery = 67% Analysis Date = 06/28/17 Pct Recovery = 67% Analysis Date = 06/18/17 Pct Recovery = 66% Analysis Date = 06/18/17 Pct Recovery = 66% Analysis Date = 06/08/17 Pct Recovery = 66% Analysis Date = 06/08/17 Pct Recovery = 66% Analysis Date = 05/29/17 Pct Recovery = 66% Analysis Date = 05/29/17 Pct Recovery = 66% Analysis Date = 05/19/17 Pct Recovery = 66% Analysis Date = 05/19/17 Pct Recovery = 66% Analysis Date = 05/09/17 Pct Recovery = 66% Analysis Date = 05/09/17 Pct Recovery = 66% Analysis Date = 04/29/17 Pct Recovery = 66% Analysis Date = 04/29/17 Pct Recovery = 66% Analysis Date = 04/19/17 Pct Recovery = 66% Analysis Date = 04/19/17 Pct Recovery = 66% Analysis Date = 04/09/17 Pct Recovery = 66% Analysis Date = 04/09/17 Pct Recovery = 66% Analysis Date = 03/31/17 Pct Recovery = 66% Analysis Date = 03/31/17 Pct Recovery = 66% Analysis Date = 03/21/17 Pct Recovery = 66% Analysis Date = 03/21/17 Pct Recovery = 66% Analysis Date = 03/11/17 Pct Recovery = 66% Analysis Date = 03/11/17 Pct Recovery = 66% Analysis Date = 03/01/17 Pct Recovery = 66% Analysis Date = 03/01/17 Pct Recovery = 66% Analysis Date = 02/19/17 Pct Recovery = 66% Analysis Date = 02/19/17 Pct Recovery = 66% Analysis Date = 02/09/17 Pct Recovery = 66% Analysis Date = 02/09/17 Pct Recovery = 66% Analysis Date = 01/30/17 Pct Recovery = 66% Analysis Date = 01/30/17 Pct Recovery = 66% Analysis Date = 01/20/17 Pct Recovery = 66% Analysis Date = 01/20/17 Pct Recovery = 66% Analysis Date = 01/10/17 Pct Recovery = 65% Analysis Date = 01/10/17 Pct Recovery = 65% Analysis Date = 12/31/16 Pct Recovery = 65% Analysis Date = 12/31/16 Pct Recovery = 65% Analysis Date = 12/21/16 Pct Recovery = 65% Analysis Date = 12/21/16 Pct Recovery = 65% Analysis Date = 12/12/16 Pct Recovery = 65% Analysis Date = 12/12/16 Pct Recovery = 65% Analysis Date = 12/02/16 Pct Recovery = 65% Analysis Date = 12/02/16 Pct Recovery = 65% Analysis Date = 11/22/16 Pct Recovery = 65% Analysis Date = 11/22/16 Pct Recovery = 65% Analysis Date = 11/12/16 Pct Recovery = 65% Analysis Date = 11/12/16 Pct Recovery = 65% Analysis Date = 11/02/16 Pct Recovery = 65% Analysis Date = 11/02/16 Pct Recovery = 65% Analysis Date = 10/23/16 Pct Recovery = 65% Analysis Date = 10/23/16 Pct Recovery = 65% Analysis Date = 10/13/16 Pct Recovery = 65% Analysis Date = 10/13/16 Pct Recovery = 65% Analysis Date = 10/03/16 Pct Recovery = 65% Analysis Date = 10/03/16 Pct Recovery = 65% Analysis Date = 09/23/16 Pct Recovery = 65% Analysis Date = 09/23/16 Pct Recovery = 65% Analysis Date = 09/13/16 Pct Recovery = 65% Analysis Date = 09/13/16 Pct Recovery = 65% Analysis Date = 09/03/16 Pct Recovery = 65% Analysis Date = 09/03/16 Pct Recovery = 65% Analysis Date = 08/25/16 Pct Recovery = 65% Analysis Date = 08/25/16 Pct Recovery = 65% Analysis Date = 08/15/16 Pct Recovery = 65% Analysis Date = 08/15/16 Pct Recovery = 65% Analysis Date = 08/05/16 Pct Recovery = 65% Analysis Date = 08/05/16 Pct Recovery = 65% Analysis Date = 07/26/16 Pct Recovery = 65% Analysis Date = 07/26/16 Pct Recovery = 65% Analysis Date = 07/16/16 Pct Recovery = 65% Analysis Date = 07/16/16 Pct Recovery = 65% Analysis Date = 07/06/16 Pct Recovery = 65% Analysis Date = 07/06/16 Pct Recovery = 65% Analysis Date = 06/26/16 Pct Recovery = 65% Analysis Date = 06/26/16 Pct Recovery = 65% Analysis Date = 06/16/16 Pct Recovery = 65% Analysis Date = 06/16/16 Pct Recovery = 65% Analysis Date = 06/06/16 Pct Recovery = 66% Analysis Date = 06/06/16 Pct Recovery = 66% Analysis Date = 05/27/16 Pct Recovery = 66% Analysis Date = 05/27/16 Pct Recovery = 66% Analysis Date = 05/17/16 Pct Recovery = 66% Analysis Date = 05/17/16 Pct Recovery = 66% Analysis Date = 05/08/16 Pct Recovery = 66% Analysis Date = 05/08/16 Pct Recovery = 66% Analysis Date = 04/28/16 Pct Recovery = 66% Analysis Date = 04/28/16 Pct Recovery = 66% Analysis Date = 04/18/16 Pct Recovery = 67% Analysis Date = 04/18/16 Pct Recovery = 67% Analysis Date = 04/08/16 Pct Recovery = 67% Analysis Date = 04/08/16 Pct Recovery = 67% Analysis Date = 03/29/16 Pct Recovery = 67% Analysis Date = 03/29/16 Pct Recovery = 67% Analysis Date = 03/19/16 Pct Recovery = 67% Analysis Date = 03/19/16 Pct Recovery = 67% Analysis Date = 03/09/16 Pct Recovery = 68% Analysis Date = 03/09/16 Pct Recovery = 68% Analysis Date = 02/28/16 Pct Recovery = 68% Analysis Date = 02/28/16 Pct Recovery = 68% Analysis Date = 02/18/16 Pct Recovery = 68% Analysis Date = 02/18/16 Pct Recovery = 68% Analysis Date = 02/08/16 Pct Recovery = 69% Analysis Date = 02/08/16 Pct Recovery = 69% Analysis Date = 01/29/16 Pct Recovery = 69% Analysis Date = 01/29/16 Pct Recovery = 69% Analysis Date = 01/20/16 Pct Recovery = 69% Analysis Date = 01/20/16 Pct Recovery = 69% Analysis Date = 01/10/16 Pct Recovery = 69% Analysis Date = 01/10/16 Pct Recovery = 69% Analysis Date = 12/31/15 Pct Recovery = 69% Analysis Date = 12/31/15 Pct Recovery = 69% Analysis Date = 12/21/15 Pct Recovery = 69% Analysis Date = 12/21/15 Pct Recovery = 69% Analysis Date = 12/11/15 Pct Recovery = 69% Analysis Date = 12/11/15 Pct Recovery = 69% Analysis Date = 12/01/15 Pct Recovery = 69% Analysis Date = 12/01/15 Pct Recovery = 69% Analysis Date = 11/21/15 Pct Recovery = 70% Analysis Date = 11/21/15 Pct Recovery = 70% Analysis Date = 11/11/15 Pct Recovery = 70% Analysis Date = 11/11/15 Pct Recovery = 70% Analysis Date = 11/01/15 Pct Recovery = 70% Analysis Date = 11/01/15 Pct Recovery = 70% Analysis Date = 10/22/15 Pct Recovery = 70% Analysis Date = 10/22/15 Pct Recovery = 70% Analysis Date = 10/12/15 Pct Recovery = 70% Analysis Date = 10/12/15 Pct Recovery = 70% Analysis Date = 10/02/15 Pct Recovery = 70% Analysis Date = 10/02/15 Pct Recovery = 70% Analysis Date = 09/23/15 Pct Recovery = 70% Analysis Date = 09/23/15 Pct Recovery = 70% Analysis Date = 09/13/15 Pct Recovery = 70% Analysis Date = 09/13/15 Pct Recovery = 70% Analysis Date = 09/03/15 Pct Recovery = 70% Analysis Date = 09/03/15 Pct Recovery = 70% Analysis Date = 08/24/15 Pct Recovery = 70% Analysis Date = 08/24/15 Pct Recovery = 70% Analysis Date = 08/14/15 Pct Recovery = 69% Analysis Date = 08/14/15 Pct Recovery = 69% Analysis Date = 08/04/15 Pct Recovery = 69% Analysis Date = 08/04/15 Pct Recovery = 69% Analysis Date = 07/25/15 Pct Recovery = 69% Analysis Date = 07/25/15 Pct Recovery = 69% Analysis Date = 07/15/15 Pct Recovery = 69% Analysis Date = 07/15/15 Pct Recovery = 69% Analysis Date = 07/05/15 Pct Recovery = 69% Analysis Date = 07/05/15 Pct Recovery = 69% Analysis Date = 06/25/15 Pct Recovery = 69% Analysis Date = 06/25/15 Pct Recovery = 69% Analysis Date = 06/15/15 Pct Recovery = 68% Analysis Date = 06/15/15 Pct Recovery = 68% Analysis Date = 06/06/15 Pct Recovery = 68% Analysis Date = 06/06/15 Pct Recovery = 68% Analysis Date = 05/27/15 Pct Recovery = 68% Analysis Date = 05/27/15 Pct Recovery = 68% Analysis Date = 05/17/15 Pct Recovery = 68% Analysis Date = 05/17/15 Pct Recovery = 68% Analysis Date = 05/07/15 Pct Recovery = 68% Analysis Date = 05/07/15 Pct Recovery = 68% Analysis Date = 04/27/15 Pct Recovery = 68% Analysis Date = 04/27/15 Pct Recovery = 68% Analysis Date = 04/17/15 Pct Recovery = 68% Analysis Date = 04/17/15 Pct Recovery = 68% Analysis Date = 04/07/15 Pct Recovery = 68% Analysis Date = 04/07/15 Pct Recovery = 68% Analysis Date = 03/28/15 Pct Recovery = 68% Analysis Date = 03/28/15 Pct Recovery = 68% Analysis Date = 03/18/15 Pct Recovery = 68% Analysis Date = 03/18/15 Pct Recovery = 68% Analysis Date = 03/08/15 Pct Recovery = 67% Analysis Date = 03/08/15 Pct Recovery = 67% Analysis Date = 02/26/15 Pct Recovery = 67% Analysis Date = 02/26/15 Pct Recovery = 67% Analysis Date = 02/17/15 Pct Recovery = 67% Analysis Date = 02/17/15 Pct Recovery = 67% Analysis Date = 02/07/15 Pct Recovery = 67% Analysis Date = 02/07/15 Pct Recovery = 67% Analysis Date = 01/28/15 Pct Recovery = 67% Analysis Date = 01/28/15 Pct Recovery = 67% Analysis Date = 01/18/15 Pct Recovery = 67% Analysis Date = 01/18/15 Pct Recovery = 67% Analysis Date = 01/08/15 Pct Recovery = 67% Analysis Date = 01/08/15 Pct Recovery = 67% Analysis Date = 12/29/14 Pct Recovery = 67% Analysis Date = 12/29/14 Pct Recovery = 67% Analysis Date = 12/19/14 Pct Recovery = 66% Analysis Date = 12/19/14 Pct Recovery = 66% Analysis Date = 12/09/14 Pct Recovery = 66% Analysis Date = 12/09/14 Pct Recovery = 66% Analysis Date = 11/29/14 Pct Recovery = 66% Analysis Date = 11/29/14 Pct Recovery = 66% Analysis Date = 11/19/14 Pct Recovery = 66% Analysis Date = 11/19/14 Pct Recovery = 66% Analysis Date = 11/09/14 Pct Recovery = 66% Analysis Date = 11/09/14 Pct Recovery = 66% Analysis Date = 10/31/14 Pct Recovery = 66% Analysis Date = 10/31/14 Pct Recovery = 66% Analysis Date = 10/21/14 Pct Recovery = 66% Analysis Date = 10/21/14 Pct Recovery = 66% Analysis Date = 10/11/14 Pct Recovery = 66% Analysis Date = 10/11/14 Pct Recovery = 66% Analysis Date = 10/01/14 Pct Recovery = 65% Analysis Date = 10/01/14 Pct Recovery = 65% Analysis Date = 09/21/14 Pct Recovery = 65% Analysis Date = 09/21/14 Pct Recovery = 65% Analysis Date = 09/11/14 Pct Recovery = 65% Analysis Date = 09/11/14 Pct Recovery = 65% Analysis Date = 09/01/14 Pct Recovery = 65% Analysis Date = 09/01/14 Pct Recovery = 65% Analysis Date = 08/22/14 Pct Recovery = 65% Analysis Date = 08/22/14 Pct Recovery = 65% Analysis Date = 08/12/14 Pct Recovery = 65% Analysis Date = 08/12/14 Pct Recovery = 65% Analysis Date = 08/02/14 Pct Recovery = 65% Analysis Date = 08/02/14 Pct Recovery = 65% Analysis Date = 07/23/14 Pct Recovery = 64% Analysis Date = 07/23/14 Pct Recovery = 64% Analysis Date = 07/14/14 Pct Recovery = 64% Analysis Date = 07/14/14 Pct Recovery = 64% Analysis Date = 07/04/14 Pct Recovery = 64% Analysis Date = 07/04/14 Pct Recovery = 64% Analysis Date = 06/24/14 Pct Recovery = 64% Analysis Date = 06/24/14 Pct Recovery = 64% Analysis Date = 06/14/14 Pct Recovery = 64% Analysis Date = 06/14/14 Pct Recovery = 64% Analysis Date = 06/04/14 Pct Recovery = 64% Analysis Date = 06/04/14 Pct Recovery = 64% Analysis Date = 05/25/14 Pct Recovery = 64% Analysis Date = 05/25/14 Pct Recovery = 64% Analysis Date = 05/15/14 Pct Recovery = 64% Analysis Date = 05/15/14 Pct Recovery = 64% Analysis Date = 05/05/14 Pct Recovery = 64% Analysis Date = 05/05/14 Pct Recovery = 64% Analysis Date = 04/25/14 Pct Recovery = 64% Analysis Date = 04/25/14 Pct Recovery = 64% Analysis Date = 04/15/14 Pct Recovery = 63% Analysis Date = 04/15/14 Pct Recovery = 63% Analysis Date = 04/05/14 Pct Recovery = 63% Analysis Date = 04/05/14 Pct Recovery = 63% Analysis Date = 03/27/14 Pct Recovery = 63% Analysis Date = 03/27/14 Pct Recovery = 63% Analysis Date = 03/17/14 Pct Recovery = 63% Analysis Date = 03/17/14 Pct Recovery = 63% Analysis Date = 03/07/14 Pct Recovery = 63% Analysis Date = 03/07/14 Pct Recovery = 63% Analysis Date = 02/25/14 Pct Recovery = 63% Analysis Date = 02/25/14 Pct Recovery = 63% Analysis Date = 02/15/14 Pct Recovery = 63% Analysis Date = 02/15/14 Pct Recovery = 63% Analysis Date = 02/05/14 Pct Recovery = 63% Analysis Date = 02/05/14 Pct Recovery = 63% Analysis Date = 01/26/14 Pct Recovery = 63% Analysis Date = 01/26/14 Pct Recovery = 63% Analysis Date = 01/16/14 Pct Recovery = 63% Analysis Date = 01/16/14 Pct Recovery = 63% Analysis Date = 01/06/14 Pct Recovery = 63% Analysis Date = 01/06/14 Pct Recovery = 63% Analysis Date = 12/27/13 Pct Recovery = 63% Analysis Date = 12/27/13 Pct Recovery = 63% Analysis Date = 12/17/13 Pct Recovery = 62% Analysis Date = 12/17/13 Pct Recovery = 62% Analysis Date = 12/08/13 Pct Recovery = 62% Analysis Date = 12/08/13 Pct Recovery = 62% Analysis Date = 11/28/13 Pct Recovery = 62% Analysis Date = 11/28/13 Pct Recovery = 62% Analysis Date = 11/18/13 Pct Recovery = 62% Analysis Date = 11/18/13 Pct Recovery = 62% Analysis Date = 11/08/13 Pct Recovery = 62% Analysis Date = 11/08/13 Pct Recovery = 62% Analysis Date = 10/29/13 Pct Recovery = 62% Analysis Date = 10/29/13 Pct Recovery = 62% Analysis Date = 10/19/13 Pct Recovery = 62% Analysis Date = 10/19/13 Pct Recovery = 62% Analysis Date = 10/09/13 Pct Recovery = 62% Analysis Date = 10/09/13 Pct Recovery = 62% Analysis Date = 09/29/13 Pct Recovery = 62% Analysis Date = 09/29/13 Pct Recovery = 62% Analysis Date = 09/19/13 Pct Recovery = 62% Analysis Date = 09/19/13 Pct Recovery = 62% Analysis Date = 09/09/13 Pct Recovery = 62% Analysis Date = 09/09/13 Pct Recovery = 62% Analysis Date = 08/30/13 Pct Recovery = 62% Analysis Date = 08/30/13 Pct Recovery = 62% Analysis Date = 08/21/13 Pct Recovery = 62% Analysis Date = 08/21/13 Pct Recovery = 62% Analysis Date = 08/11/13 Pct Recovery = 61% Analysis Date = 08/11/13 Pct Recovery = 61% Analysis Date = 08/01/13 Pct Recovery = 61% Analysis Date = 08/01/13 Pct Recovery = 61% Analysis Date = 07/22/13 Pct Recovery = 61% Analysis Date = 07/22/13 Pct Recovery = 61% Analysis Date = 07/12/13 Pct Recovery = 61% Analysis Date = 07/12/13 Pct Recovery = 61% Analysis Date = 07/02/13 Pct Recovery = 61% Analysis Date = 07/02/13 Pct Recovery = 61% Analysis Date = 06/22/13 Pct Recovery = 61% Analysis Date = 06/22/13 Pct Recovery = 61% Analysis Date = 06/12/13 Pct Recovery = 61% Analysis Date = 06/12/13 Pct Recovery = 61% Analysis Date = 06/02/13 Pct Recovery = 61% Analysis Date = 06/02/13 Pct Recovery = 61% Analysis Date = 05/23/13 Pct Recovery = 61% Analysis Date = 05/23/13 Pct Recovery = 61% Analysis Date = 05/13/13 Pct Recovery = 61% Analysis Date = 05/13/13 Pct Recovery = 61% Analysis Date = 05/04/13 Pct Recovery = 61% Analysis Date = 05/04/13 Pct Recovery = 61% Analysis Date = 04/24/13 Pct Recovery = 61% Analysis Date = 04/24/13 Pct Recovery = 61% Analysis Date = 04/14/13 Pct Recovery = 61% Analysis Date = 04/14/13 Pct Recovery = 61% Analysis Date = 04/04/13 Pct Recovery = 61% Analysis Date = 04/04/13 Pct Recovery = 61% Analysis Date = 03/25/13 Pct Recovery = 61% Analysis Date = 03/25/13 Pct Recovery = 61% Analysis Date = 03/15/13 Pct Recovery = 61% Analysis Date = 03/15/13 Pct Recovery = 61% Analysis Date = 03/05/13 Pct Recovery = 61% Analysis Date = 03/05/13 Pct Recovery = 61% Analysis Date = 02/23/13 Pct Recovery = 61% Analysis Date = 02/23/13 Pct Recovery = 61% Analysis Date = 02/13/13 Pct Recovery = 61% Analysis Date = 02/13/13 Pct Recovery = 61% Analysis Date = 02/03/13 Pct Recovery = 61% Analysis Date = 02/03/13 Pct Recovery = 61% Analysis Date = 01/24/13 Pct Recovery = 61% Analysis Date = 01/24/13 Pct Recovery = 61% Analysis Date = 01/15/13 Pct Recovery = 61% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
CIS-PERMETHRIN

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 72 65% 21% 63% 22%
Total 72 65% 21% 63% 22%

Sample Statistics
CIS-PERMETHRIN

Characteristic N % % Basis
Plotted 72 100% Spiked
Estimated Values 5 7% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 72 .  
False Negatives 0 0% 0 out of 72
Not Spiked 58 .  
False Positives 0 0% 0 out of 58

OBSP Determination:
CYANAZINE
METHOD: 2033 , TESTIDCODE: 04041GCM35

Laboratory ID = 20140100085 Lab Value = 0.293 Expected Conc. = 0.276 Report level label = 0.022 Pct Recovery = 106% Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl SpecificMix = 042413 Laboratory ID = 20130250061 Lab Value = 0.136 Expected Conc. = 0.149 Report level label = 0.022 Pct Recovery = 91% Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl SpecificMix = 05BB029 Laboratory ID = 20172510330 Lab Value = 0.140 Expected Conc. = 0.147 Report level label = 0.022 Pct Recovery = 95% Analysis Date = 12/29/17 SpikeMix = ChemService 6537100: 100 µl & Abs 071817Pest: 100 µl SpecificMix = 071817Pest Laboratory ID = 20162860079 Lab Value = 0.140 Expected Conc. = 0.139 Report level label = 0.022 Pct Recovery = 101% Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl SpecificMix = 060916 Laboratory ID = 20163150006 Lab Value = 0.120 Expected Conc. = 0.139 Report level label = 0.022 Pct Recovery = 86% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl SpecificMix = 060916 Laboratory ID = 20132690010 Lab Value = 0.139 Expected Conc. = 0.138 Report level label = 0.022 Pct Recovery = 101% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl SpecificMix = 042413 Laboratory ID = 20132560001 Lab Value = 0.122 Expected Conc. = 0.138 Report level label = 0.022 Pct Recovery = 88% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl SpecificMix = 042413 Laboratory ID = 20132140002 Lab Value = 0.117 Expected Conc. = 0.137 Report level label = 0.022 Pct Recovery = 85% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl SpecificMix = 04CC101 Laboratory ID = 20152610011 Lab Value = 0.030 Expected Conc. = 0.132 Report level label = 0.022 Pct Recovery = 23% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl SpecificMix = 0406-15-01 Laboratory ID = 20152460215 Lab Value = 0.101 Expected Conc. = 0.132 Report level label = 0.022 Pct Recovery = 77% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl SpecificMix = 0406-15-01 Laboratory ID = 20171380001 Lab Value = 0.069 Expected Conc. = 0.1136 Report level label = 0.022 Pct Recovery = 60% Analysis Date = 06/07/17 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 041816 Laboratory ID = 20170740063 Lab Value = 0.024 Expected Conc. = 0.1136 Report level label = 0.022 Pct Recovery = 21% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl SpecificMix = 041816 Laboratory ID = 20161740258 Lab Value = 0.077 Expected Conc. = 0.1136 Report level label = 0.022 Pct Recovery = 68% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 041816 Laboratory ID = 20171660002 Lab Value = 0.105 Expected Conc. = 0.1112 Report level label = 0.022 Pct Recovery = 94% Analysis Date = 08/23/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = 060916 Laboratory ID = 20170190026 Lab Value = 0.105 Expected Conc. = 0.1112 Report level label = 0.022 Pct Recovery = 94% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = 060916 Laboratory ID = 20142720002 Lab Value = 0.067 Expected Conc. = 0.0884 Report level label = 0.022 Pct Recovery = 76% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl SpecificMix = LC06435 Laboratory ID = 20142530087 Lab Value = 0.059 Expected Conc. = 0.0884 Report level label = 0.022 Pct Recovery = 67% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl SpecificMix = LC06435 Laboratory ID = 20141570088 Lab Value = 0.090 Expected Conc. = 0.0884 Report level label = 0.022 Pct Recovery = 102% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl SpecificMix = LC06435 Laboratory ID = 20141220025 Lab Value = 0.089 Expected Conc. = 0.0884 Report level label = 0.022 Pct Recovery = 101% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl SpecificMix = LC06435 Laboratory ID = 20150720069 Lab Value = 0.022 Expected Conc. = 0.0876 Report level label = 0.022 Pct Recovery = 25% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 03DD006 Laboratory ID = 20143110108 Lab Value = 0.066 Expected Conc. = 0.0876 Report level label = 0.022 Pct Recovery = 75% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 03DD006 Laboratory ID = 20142960086 Lab Value = 0.069 Expected Conc. = 0.0876 Report level label = 0.022 Pct Recovery = 78% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 03DD006 Laboratory ID = 20142270001 Lab Value = 0.063 Expected Conc. = 0.0876 Report level label = 0.022 Pct Recovery = 71% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl SpecificMix = 03DD006 Laboratory ID = 20140230082 Lab Value = 0.066 Expected Conc. = 0.0755 Report level label = 0.022 Pct Recovery = 88% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl SpecificMix = 012513 Laboratory ID = 20132420001 Lab Value = 0.075 Expected Conc. = 0.0755 Report level label = 0.022 Pct Recovery = 99% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl SpecificMix = 012513 Laboratory ID = 20172560101 Lab Value = 0.054 Expected Conc. = 0.075 Report level label = 0.022 Pct Recovery = 72% Analysis Date = 12/22/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6567600: 50 µl SpecificMix = 6567600 Laboratory ID = 20130940097 Lab Value = 0.066 Expected Conc. = 0.075 Report level label = 0.022 Pct Recovery = 88% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = 052412 Laboratory ID = 20130100066 Lab Value = 0.089 Expected Conc. = 0.075 Report level label = 0.022 Pct Recovery = 119% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl SpecificMix = 052412 Laboratory ID = 20161260151 Lab Value = 0.046 Expected Conc. = 0.068 Report level label = 0.022 Pct Recovery = 67% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = 3851600 Laboratory ID = 20151550293 Lab Value = 0.066 Expected Conc. = 0.068 Report level label = 0.022 Pct Recovery = 96% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl SpecificMix = 3851600 Laboratory ID = 20151270112 Lab Value = 0.046 Expected Conc. = 0.068 Report level label = 0.022 Pct Recovery = 67% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl SpecificMix = 3851600 Laboratory ID = 20160770090 Lab Value = 0.048 Expected Conc. = 0.066 Report level label = 0.022 Pct Recovery = 73% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20160630046 Lab Value = 0.041 Expected Conc. = 0.066 Report level label = 0.022 Pct Recovery = 62% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20153510109 Lab Value = 0.052 Expected Conc. = 0.066 Report level label = 0.022 Pct Recovery = 79% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20153440001 Lab Value = 0.052 Expected Conc. = 0.066 Report level label = 0.022 Pct Recovery = 78% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20171940002 Lab Value = 0.043 Expected Conc. = 0.0568 Report level label = 0.022 Pct Recovery = 75% Analysis Date = 11/10/17 SpikeMix = ChemService 5054800: 40 µl & NSI 041816: 40 µl SpecificMix = 041816 Laboratory ID = 20162020124 Lab Value = 0.043 Expected Conc. = 0.0568 Report level label = 0.022 Pct Recovery = 76% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl SpecificMix = 041816 Laboratory ID = 20161600087 Lab Value = 0.059 Expected Conc. = 0.0568 Report level label = 0.022 Pct Recovery = 104% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 041816 Laboratory ID = 20161340228 Lab Value = 0.042 Expected Conc. = 0.0568 Report level label = 0.022 Pct Recovery = 73% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl SpecificMix = 041816 Laboratory ID = 20161190075 Lab Value = 0.038 Expected Conc. = 0.0568 Report level label = 0.022 Pct Recovery = 66% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 041816 Laboratory ID = 20171160110 Lab Value = 0.049 Expected Conc. = 0.0556 Report level label = 0.022 Pct Recovery = 88% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = 060916 Laboratory ID = 20162520001 Lab Value = 0.058 Expected Conc. = 0.0556 Report level label = 0.022 Pct Recovery = 105% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl SpecificMix = 060916 Laboratory ID = 20163560019 Lab Value = 0.046 Expected Conc. = 0.0556 Report level label = 0.022 Pct Recovery = 83% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl SpecificMix = 060916 Laboratory ID = 20162380004 Lab Value = 0.051 Expected Conc. = 0.0556 Report level label = 0.022 Pct Recovery = 92% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = 060916 Laboratory ID = 20133580036 Lab Value = 0.043 Expected Conc. = 0.0552 Report level label = 0.022 Pct Recovery = 77% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 042413 Laboratory ID = 20133190012 Lab Value = 0.065 Expected Conc. = 0.0552 Report level label = 0.022 Pct Recovery = 117% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 042413 Laboratory ID = 20131650073 Lab Value = 0.067 Expected Conc. = 0.0552 Report level label = 0.022 Pct Recovery = 120% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl SpecificMix = 042413 Laboratory ID = 20140730138 Lab Value = 0.014 Expected Conc. = 0.0548 Report level label = 0.022 Pct Recovery = 26% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 04CC101 Laboratory ID = 20140510043 Lab Value = 0.029 Expected Conc. = 0.0548 Report level label = 0.022 Pct Recovery = 52% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 04CC101 Laboratory ID = 20133310030 Lab Value = 0.059 Expected Conc. = 0.0548 Report level label = 0.022 Pct Recovery = 108% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl SpecificMix = 04CC101 Laboratory ID = 20132280016 Lab Value = 0.063 Expected Conc. = 0.0548 Report level label = 0.022 Pct Recovery = 114% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl SpecificMix = 04CC101 Laboratory ID = 20131510026 Lab Value = 0.043 Expected Conc. = 0.0548 Report level label = 0.022 Pct Recovery = 79% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl SpecificMix = 04CC101 Laboratory ID = 20150150115 Lab Value = 0.047 Expected Conc. = 0.0442 Report level label = 0.022 Pct Recovery = 107% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl SpecificMix = LC06435 Laboratory ID = 20143370094 Lab Value = 0.026 Expected Conc. = 0.0442 Report level label = 0.022 Pct Recovery = 58% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl SpecificMix = LC06435 Laboratory ID = 20141910243 Lab Value = 0.025 Expected Conc. = 0.0442 Report level label = 0.022 Pct Recovery = 56% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = LC06435 Laboratory ID = 20141840097 Lab Value = 0.028 Expected Conc. = 0.0442 Report level label = 0.022 Pct Recovery = 64% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl SpecificMix = LC06435 Laboratory ID = 20172780018 Lab Value = 0.040 Expected Conc. = 0.0441 Report level label = 0.022 Pct Recovery = 90% Analysis Date = 02/08/18 SpikeMix = ChemService 6537100: 30 µl & Abs 071817Pest: 30 µl SpecificMix = 071817Pest Laboratory ID = 20142200164 Lab Value = 0.033 Expected Conc. = 0.0438 Report level label = 0.022 Pct Recovery = 75% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 03DD006 Laboratory ID = 20141640076 Lab Value = 0.033 Expected Conc. = 0.0438 Report level label = 0.022 Pct Recovery = 76% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = 03DD006 Laboratory ID = 20141420140 Lab Value = 0.040 Expected Conc. = 0.0438 Report level label = 0.022 Pct Recovery = 92% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 03DD006 Laboratory ID = 20141080004 Lab Value = 0.036 Expected Conc. = 0.0438 Report level label = 0.022 Pct Recovery = 81% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl SpecificMix = 03DD006 Laboratory ID = 20160430111 Lab Value = 0.027 Expected Conc. = 0.034 Report level label = 0.022 Pct Recovery = 79% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 3851600 Laboratory ID = 20160210080 Lab Value = 0.019 Expected Conc. = 0.034 Report level label = 0.022 Pct Recovery = 56% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 3851600 Laboratory ID = 20152950078 Lab Value = 0.017 Expected Conc. = 0.034 Report level label = 0.022 Pct Recovery = 49% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 3851600 Laboratory ID = 20153030068 Lab Value = 0.026 Expected Conc. = 0.034 Report level label = 0.022 Pct Recovery = 76% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = 3851600 Laboratory ID = 20151760208 Lab Value = 0.044 Expected Conc. = 0.034 Report level label = 0.022 Pct Recovery = 129% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl SpecificMix = 3851600 Laboratory ID = 20151380009 Lab Value = 0.024 Expected Conc. = 0.034 Report level label = 0.022 Pct Recovery = 69% Analysis Date = 05/30/15 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 3851600 Laboratory ID = 20152190003 Lab Value = 0.027 Expected Conc. = 0.033 Report level label = 0.022 Pct Recovery = 83% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = 0406-15-01 Laboratory ID = 20152040177 Lab Value = 0.034 Expected Conc. = 0.033 Report level label = 0.022 Pct Recovery = 102% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl SpecificMix = 0406-15-01 Laboratory ID = 20140860102 Lab Value = 0.026 Expected Conc. = 0.0302 Report level label = 0.022 Pct Recovery = 87% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 012513 Laboratory ID = 20131920149 Lab Value = 0.032 Expected Conc. = 0.0302 Report level label = 0.022 Pct Recovery = 107% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl SpecificMix = 012513 Laboratory ID = 20133400002 Lab Value = 0.032 Expected Conc. = 0.03 Report level label = 0.022 Pct Recovery = 107% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = 052412 Laboratory ID = 20132910008 Lab Value = 0.027 Expected Conc. = 0.03 Report level label = 0.022 Pct Recovery = 91% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = 052412 Laboratory ID = 20130650005 Lab Value = 0.023 Expected Conc. = 0.03 Report level label = 0.022 Pct Recovery = 77% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl SpecificMix = 052412 Laboratory ID = 20131230084 Lab Value = 0.041 Expected Conc. = 0.0298 Report level label = 0.022 Pct Recovery = 136% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl SpecificMix = 05BB029 Laboratory ID = 20130510051 Lab Value = 0.026 Expected Conc. = 0.0298 Report level label = 0.022 Pct Recovery = 88% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl SpecificMix = 05BB029 Analysis Date = 02/08/18 Pct Recovery = 85% Analysis Date = 01/29/18 Pct Recovery = 85% Analysis Date = 01/29/18 Pct Recovery = 85% Analysis Date = 01/20/18 Pct Recovery = 85% Analysis Date = 01/20/18 Pct Recovery = 85% Analysis Date = 01/11/18 Pct Recovery = 85% Analysis Date = 01/11/18 Pct Recovery = 85% Analysis Date = 01/02/18 Pct Recovery = 85% Analysis Date = 01/02/18 Pct Recovery = 85% Analysis Date = 12/23/17 Pct Recovery = 85% Analysis Date = 12/23/17 Pct Recovery = 85% Analysis Date = 12/14/17 Pct Recovery = 84% Analysis Date = 12/14/17 Pct Recovery = 84% Analysis Date = 12/05/17 Pct Recovery = 84% Analysis Date = 12/05/17 Pct Recovery = 84% Analysis Date = 11/26/17 Pct Recovery = 84% Analysis Date = 11/26/17 Pct Recovery = 84% Analysis Date = 11/16/17 Pct Recovery = 84% Analysis Date = 11/16/17 Pct Recovery = 84% Analysis Date = 11/07/17 Pct Recovery = 84% Analysis Date = 11/07/17 Pct Recovery = 84% Analysis Date = 10/29/17 Pct Recovery = 84% Analysis Date = 10/29/17 Pct Recovery = 84% Analysis Date = 10/20/17 Pct Recovery = 84% Analysis Date = 10/20/17 Pct Recovery = 84% Analysis Date = 10/10/17 Pct Recovery = 83% Analysis Date = 10/10/17 Pct Recovery = 83% Analysis Date = 10/01/17 Pct Recovery = 83% Analysis Date = 10/01/17 Pct Recovery = 83% Analysis Date = 09/22/17 Pct Recovery = 83% Analysis Date = 09/22/17 Pct Recovery = 83% Analysis Date = 09/13/17 Pct Recovery = 83% Analysis Date = 09/13/17 Pct Recovery = 83% Analysis Date = 09/03/17 Pct Recovery = 83% Analysis Date = 09/03/17 Pct Recovery = 83% Analysis Date = 08/25/17 Pct Recovery = 83% Analysis Date = 08/25/17 Pct Recovery = 83% Analysis Date = 08/16/17 Pct Recovery = 82% Analysis Date = 08/16/17 Pct Recovery = 82% Analysis Date = 08/07/17 Pct Recovery = 82% Analysis Date = 08/07/17 Pct Recovery = 82% Analysis Date = 07/28/17 Pct Recovery = 82% Analysis Date = 07/28/17 Pct Recovery = 82% Analysis Date = 07/19/17 Pct Recovery = 82% Analysis Date = 07/19/17 Pct Recovery = 82% Analysis Date = 07/10/17 Pct Recovery = 82% Analysis Date = 07/10/17 Pct Recovery = 82% Analysis Date = 07/01/17 Pct Recovery = 82% Analysis Date = 07/01/17 Pct Recovery = 82% Analysis Date = 06/22/17 Pct Recovery = 82% Analysis Date = 06/22/17 Pct Recovery = 82% Analysis Date = 06/12/17 Pct Recovery = 81% Analysis Date = 06/12/17 Pct Recovery = 81% Analysis Date = 06/03/17 Pct Recovery = 81% Analysis Date = 06/03/17 Pct Recovery = 81% Analysis Date = 05/25/17 Pct Recovery = 81% Analysis Date = 05/25/17 Pct Recovery = 81% Analysis Date = 05/16/17 Pct Recovery = 81% Analysis Date = 05/16/17 Pct Recovery = 81% Analysis Date = 05/06/17 Pct Recovery = 81% Analysis Date = 05/06/17 Pct Recovery = 81% Analysis Date = 04/27/17 Pct Recovery = 81% Analysis Date = 04/27/17 Pct Recovery = 81% Analysis Date = 04/18/17 Pct Recovery = 81% Analysis Date = 04/18/17 Pct Recovery = 81% Analysis Date = 04/09/17 Pct Recovery = 80% Analysis Date = 04/09/17 Pct Recovery = 80% Analysis Date = 03/30/17 Pct Recovery = 80% Analysis Date = 03/30/17 Pct Recovery = 80% Analysis Date = 03/21/17 Pct Recovery = 80% Analysis Date = 03/21/17 Pct Recovery = 80% Analysis Date = 03/12/17 Pct Recovery = 80% Analysis Date = 03/12/17 Pct Recovery = 80% Analysis Date = 03/03/17 Pct Recovery = 80% Analysis Date = 03/03/17 Pct Recovery = 80% Analysis Date = 02/21/17 Pct Recovery = 80% Analysis Date = 02/21/17 Pct Recovery = 80% Analysis Date = 02/12/17 Pct Recovery = 80% Analysis Date = 02/12/17 Pct Recovery = 80% Analysis Date = 02/03/17 Pct Recovery = 79% Analysis Date = 02/03/17 Pct Recovery = 79% Analysis Date = 01/25/17 Pct Recovery = 79% Analysis Date = 01/25/17 Pct Recovery = 79% Analysis Date = 01/15/17 Pct Recovery = 79% Analysis Date = 01/15/17 Pct Recovery = 79% Analysis Date = 01/06/17 Pct Recovery = 79% Analysis Date = 01/06/17 Pct Recovery = 79% Analysis Date = 12/28/16 Pct Recovery = 79% Analysis Date = 12/28/16 Pct Recovery = 79% Analysis Date = 12/19/16 Pct Recovery = 79% Analysis Date = 12/19/16 Pct Recovery = 79% Analysis Date = 12/09/16 Pct Recovery = 79% Analysis Date = 12/09/16 Pct Recovery = 79% Analysis Date = 11/30/16 Pct Recovery = 78% Analysis Date = 11/30/16 Pct Recovery = 78% Analysis Date = 11/21/16 Pct Recovery = 78% Analysis Date = 11/21/16 Pct Recovery = 78% Analysis Date = 11/12/16 Pct Recovery = 78% Analysis Date = 11/12/16 Pct Recovery = 78% Analysis Date = 11/03/16 Pct Recovery = 78% Analysis Date = 11/03/16 Pct Recovery = 78% Analysis Date = 10/24/16 Pct Recovery = 78% Analysis Date = 10/24/16 Pct Recovery = 78% Analysis Date = 10/15/16 Pct Recovery = 78% Analysis Date = 10/15/16 Pct Recovery = 78% Analysis Date = 10/06/16 Pct Recovery = 78% Analysis Date = 10/06/16 Pct Recovery = 78% Analysis Date = 09/27/16 Pct Recovery = 78% Analysis Date = 09/27/16 Pct Recovery = 78% Analysis Date = 09/17/16 Pct Recovery = 77% Analysis Date = 09/17/16 Pct Recovery = 77% Analysis Date = 09/08/16 Pct Recovery = 77% Analysis Date = 09/08/16 Pct Recovery = 77% Analysis Date = 08/30/16 Pct Recovery = 77% Analysis Date = 08/30/16 Pct Recovery = 77% Analysis Date = 08/21/16 Pct Recovery = 77% Analysis Date = 08/21/16 Pct Recovery = 77% Analysis Date = 08/11/16 Pct Recovery = 77% Analysis Date = 08/11/16 Pct Recovery = 77% Analysis Date = 08/02/16 Pct Recovery = 77% Analysis Date = 08/02/16 Pct Recovery = 77% Analysis Date = 07/24/16 Pct Recovery = 77% Analysis Date = 07/24/16 Pct Recovery = 77% Analysis Date = 07/15/16 Pct Recovery = 77% Analysis Date = 07/15/16 Pct Recovery = 77% Analysis Date = 07/05/16 Pct Recovery = 76% Analysis Date = 07/05/16 Pct Recovery = 76% Analysis Date = 06/26/16 Pct Recovery = 76% Analysis Date = 06/26/16 Pct Recovery = 76% Analysis Date = 06/17/16 Pct Recovery = 76% Analysis Date = 06/17/16 Pct Recovery = 76% Analysis Date = 06/08/16 Pct Recovery = 76% Analysis Date = 06/08/16 Pct Recovery = 76% Analysis Date = 05/29/16 Pct Recovery = 76% Analysis Date = 05/29/16 Pct Recovery = 76% Analysis Date = 05/20/16 Pct Recovery = 76% Analysis Date = 05/20/16 Pct Recovery = 76% Analysis Date = 05/11/16 Pct Recovery = 76% Analysis Date = 05/11/16 Pct Recovery = 76% Analysis Date = 05/02/16 Pct Recovery = 76% Analysis Date = 05/02/16 Pct Recovery = 76% Analysis Date = 04/22/16 Pct Recovery = 76% Analysis Date = 04/22/16 Pct Recovery = 76% Analysis Date = 04/13/16 Pct Recovery = 76% Analysis Date = 04/13/16 Pct Recovery = 76% Analysis Date = 04/04/16 Pct Recovery = 75% Analysis Date = 04/04/16 Pct Recovery = 75% Analysis Date = 03/26/16 Pct Recovery = 75% Analysis Date = 03/26/16 Pct Recovery = 75% Analysis Date = 03/17/16 Pct Recovery = 75% Analysis Date = 03/17/16 Pct Recovery = 75% Analysis Date = 03/07/16 Pct Recovery = 75% Analysis Date = 03/07/16 Pct Recovery = 75% Analysis Date = 02/27/16 Pct Recovery = 75% Analysis Date = 02/27/16 Pct Recovery = 75% Analysis Date = 02/18/16 Pct Recovery = 75% Analysis Date = 02/18/16 Pct Recovery = 75% Analysis Date = 02/09/16 Pct Recovery = 75% Analysis Date = 02/09/16 Pct Recovery = 75% Analysis Date = 01/30/16 Pct Recovery = 75% Analysis Date = 01/30/16 Pct Recovery = 75% Analysis Date = 01/21/16 Pct Recovery = 75% Analysis Date = 01/21/16 Pct Recovery = 75% Analysis Date = 01/12/16 Pct Recovery = 75% Analysis Date = 01/12/16 Pct Recovery = 75% Analysis Date = 01/03/16 Pct Recovery = 75% Analysis Date = 01/03/16 Pct Recovery = 75% Analysis Date = 12/24/15 Pct Recovery = 74% Analysis Date = 12/24/15 Pct Recovery = 74% Analysis Date = 12/15/15 Pct Recovery = 74% Analysis Date = 12/15/15 Pct Recovery = 74% Analysis Date = 12/06/15 Pct Recovery = 74% Analysis Date = 12/06/15 Pct Recovery = 74% Analysis Date = 11/27/15 Pct Recovery = 74% Analysis Date = 11/27/15 Pct Recovery = 74% Analysis Date = 11/17/15 Pct Recovery = 74% Analysis Date = 11/17/15 Pct Recovery = 74% Analysis Date = 11/08/15 Pct Recovery = 74% Analysis Date = 11/08/15 Pct Recovery = 74% Analysis Date = 10/30/15 Pct Recovery = 74% Analysis Date = 10/30/15 Pct Recovery = 74% Analysis Date = 10/21/15 Pct Recovery = 74% Analysis Date = 10/21/15 Pct Recovery = 74% Analysis Date = 10/11/15 Pct Recovery = 74% Analysis Date = 10/11/15 Pct Recovery = 74% Analysis Date = 10/02/15 Pct Recovery = 74% Analysis Date = 10/02/15 Pct Recovery = 74% Analysis Date = 09/23/15 Pct Recovery = 74% Analysis Date = 09/23/15 Pct Recovery = 74% Analysis Date = 09/14/15 Pct Recovery = 74% Analysis Date = 09/14/15 Pct Recovery = 74% Analysis Date = 09/04/15 Pct Recovery = 74% Analysis Date = 09/04/15 Pct Recovery = 74% Analysis Date = 08/26/15 Pct Recovery = 74% Analysis Date = 08/26/15 Pct Recovery = 74% Analysis Date = 08/17/15 Pct Recovery = 74% Analysis Date = 08/17/15 Pct Recovery = 74% Analysis Date = 08/08/15 Pct Recovery = 74% Analysis Date = 08/08/15 Pct Recovery = 74% Analysis Date = 07/30/15 Pct Recovery = 74% Analysis Date = 07/30/15 Pct Recovery = 74% Analysis Date = 07/20/15 Pct Recovery = 74% Analysis Date = 07/20/15 Pct Recovery = 74% Analysis Date = 07/11/15 Pct Recovery = 74% Analysis Date = 07/11/15 Pct Recovery = 74% Analysis Date = 07/02/15 Pct Recovery = 74% Analysis Date = 07/02/15 Pct Recovery = 74% Analysis Date = 06/23/15 Pct Recovery = 74% Analysis Date = 06/23/15 Pct Recovery = 74% Analysis Date = 06/13/15 Pct Recovery = 74% Analysis Date = 06/13/15 Pct Recovery = 74% Analysis Date = 06/04/15 Pct Recovery = 74% Analysis Date = 06/04/15 Pct Recovery = 74% Analysis Date = 05/26/15 Pct Recovery = 74% Analysis Date = 05/26/15 Pct Recovery = 74% Analysis Date = 05/17/15 Pct Recovery = 74% Analysis Date = 05/17/15 Pct Recovery = 74% Analysis Date = 05/07/15 Pct Recovery = 74% Analysis Date = 05/07/15 Pct Recovery = 74% Analysis Date = 04/28/15 Pct Recovery = 75% Analysis Date = 04/28/15 Pct Recovery = 75% Analysis Date = 04/19/15 Pct Recovery = 75% Analysis Date = 04/19/15 Pct Recovery = 75% Analysis Date = 04/10/15 Pct Recovery = 75% Analysis Date = 04/10/15 Pct Recovery = 75% Analysis Date = 03/31/15 Pct Recovery = 75% Analysis Date = 03/31/15 Pct Recovery = 75% Analysis Date = 03/22/15 Pct Recovery = 75% Analysis Date = 03/22/15 Pct Recovery = 75% Analysis Date = 03/13/15 Pct Recovery = 75% Analysis Date = 03/13/15 Pct Recovery = 75% Analysis Date = 03/04/15 Pct Recovery = 75% Analysis Date = 03/04/15 Pct Recovery = 75% Analysis Date = 02/22/15 Pct Recovery = 75% Analysis Date = 02/22/15 Pct Recovery = 75% Analysis Date = 02/13/15 Pct Recovery = 76% Analysis Date = 02/13/15 Pct Recovery = 76% Analysis Date = 02/04/15 Pct Recovery = 76% Analysis Date = 02/04/15 Pct Recovery = 76% Analysis Date = 01/26/15 Pct Recovery = 76% Analysis Date = 01/26/15 Pct Recovery = 76% Analysis Date = 01/16/15 Pct Recovery = 76% Analysis Date = 01/16/15 Pct Recovery = 76% Analysis Date = 01/07/15 Pct Recovery = 76% Analysis Date = 01/07/15 Pct Recovery = 76% Analysis Date = 12/29/14 Pct Recovery = 76% Analysis Date = 12/29/14 Pct Recovery = 76% Analysis Date = 12/20/14 Pct Recovery = 76% Analysis Date = 12/20/14 Pct Recovery = 76% Analysis Date = 12/11/14 Pct Recovery = 77% Analysis Date = 12/11/14 Pct Recovery = 77% Analysis Date = 12/01/14 Pct Recovery = 77% Analysis Date = 12/01/14 Pct Recovery = 77% Analysis Date = 11/22/14 Pct Recovery = 77% Analysis Date = 11/22/14 Pct Recovery = 77% Analysis Date = 11/13/14 Pct Recovery = 77% Analysis Date = 11/13/14 Pct Recovery = 77% Analysis Date = 11/04/14 Pct Recovery = 77% Analysis Date = 11/04/14 Pct Recovery = 77% Analysis Date = 10/25/14 Pct Recovery = 77% Analysis Date = 10/25/14 Pct Recovery = 77% Analysis Date = 10/16/14 Pct Recovery = 78% Analysis Date = 10/16/14 Pct Recovery = 78% Analysis Date = 10/07/14 Pct Recovery = 78% Analysis Date = 10/07/14 Pct Recovery = 78% Analysis Date = 09/28/14 Pct Recovery = 78% Analysis Date = 09/28/14 Pct Recovery = 78% Analysis Date = 09/18/14 Pct Recovery = 78% Analysis Date = 09/18/14 Pct Recovery = 78% Analysis Date = 09/09/14 Pct Recovery = 78% Analysis Date = 09/09/14 Pct Recovery = 78% Analysis Date = 08/31/14 Pct Recovery = 78% Analysis Date = 08/31/14 Pct Recovery = 78% Analysis Date = 08/22/14 Pct Recovery = 79% Analysis Date = 08/22/14 Pct Recovery = 79% Analysis Date = 08/12/14 Pct Recovery = 79% Analysis Date = 08/12/14 Pct Recovery = 79% Analysis Date = 08/03/14 Pct Recovery = 79% Analysis Date = 08/03/14 Pct Recovery = 79% Analysis Date = 07/25/14 Pct Recovery = 79% Analysis Date = 07/25/14 Pct Recovery = 79% Analysis Date = 07/16/14 Pct Recovery = 79% Analysis Date = 07/16/14 Pct Recovery = 79% Analysis Date = 07/06/14 Pct Recovery = 79% Analysis Date = 07/06/14 Pct Recovery = 79% Analysis Date = 06/27/14 Pct Recovery = 80% Analysis Date = 06/27/14 Pct Recovery = 80% Analysis Date = 06/18/14 Pct Recovery = 80% Analysis Date = 06/18/14 Pct Recovery = 80% Analysis Date = 06/09/14 Pct Recovery = 81% Analysis Date = 06/09/14 Pct Recovery = 81% Analysis Date = 05/30/14 Pct Recovery = 81% Analysis Date = 05/30/14 Pct Recovery = 81% Analysis Date = 05/21/14 Pct Recovery = 82% Analysis Date = 05/21/14 Pct Recovery = 82% Analysis Date = 05/12/14 Pct Recovery = 82% Analysis Date = 05/12/14 Pct Recovery = 82% Analysis Date = 05/03/14 Pct Recovery = 83% Analysis Date = 05/03/14 Pct Recovery = 83% Analysis Date = 04/24/14 Pct Recovery = 83% Analysis Date = 04/24/14 Pct Recovery = 83% Analysis Date = 04/14/14 Pct Recovery = 83% Analysis Date = 04/14/14 Pct Recovery = 83% Analysis Date = 04/05/14 Pct Recovery = 84% Analysis Date = 04/05/14 Pct Recovery = 84% Analysis Date = 03/27/14 Pct Recovery = 84% Analysis Date = 03/27/14 Pct Recovery = 84% Analysis Date = 03/18/14 Pct Recovery = 85% Analysis Date = 03/18/14 Pct Recovery = 85% Analysis Date = 03/08/14 Pct Recovery = 85% Analysis Date = 03/08/14 Pct Recovery = 85% Analysis Date = 02/27/14 Pct Recovery = 86% Analysis Date = 02/27/14 Pct Recovery = 86% Analysis Date = 02/18/14 Pct Recovery = 86% Analysis Date = 02/18/14 Pct Recovery = 86% Analysis Date = 02/09/14 Pct Recovery = 87% Analysis Date = 02/09/14 Pct Recovery = 87% Analysis Date = 01/30/14 Pct Recovery = 87% Analysis Date = 01/30/14 Pct Recovery = 87% Analysis Date = 01/21/14 Pct Recovery = 88% Analysis Date = 01/21/14 Pct Recovery = 88% Analysis Date = 01/12/14 Pct Recovery = 88% Analysis Date = 01/12/14 Pct Recovery = 88% Analysis Date = 01/03/14 Pct Recovery = 89% Analysis Date = 01/03/14 Pct Recovery = 89% Analysis Date = 12/24/13 Pct Recovery = 89% Analysis Date = 12/24/13 Pct Recovery = 89% Analysis Date = 12/15/13 Pct Recovery = 90% Analysis Date = 12/15/13 Pct Recovery = 90% Analysis Date = 12/06/13 Pct Recovery = 90% Analysis Date = 12/06/13 Pct Recovery = 90% Analysis Date = 11/27/13 Pct Recovery = 91% Analysis Date = 11/27/13 Pct Recovery = 91% Analysis Date = 11/17/13 Pct Recovery = 91% Analysis Date = 11/17/13 Pct Recovery = 91% Analysis Date = 11/08/13 Pct Recovery = 92% Analysis Date = 11/08/13 Pct Recovery = 92% Analysis Date = 10/30/13 Pct Recovery = 92% Analysis Date = 10/30/13 Pct Recovery = 92% Analysis Date = 10/21/13 Pct Recovery = 93% Analysis Date = 10/21/13 Pct Recovery = 93% Analysis Date = 10/11/13 Pct Recovery = 93% Analysis Date = 10/11/13 Pct Recovery = 93% Analysis Date = 10/02/13 Pct Recovery = 94% Analysis Date = 10/02/13 Pct Recovery = 94% Analysis Date = 09/23/13 Pct Recovery = 94% Analysis Date = 09/23/13 Pct Recovery = 94% Analysis Date = 09/14/13 Pct Recovery = 95% Analysis Date = 09/14/13 Pct Recovery = 95% Analysis Date = 09/05/13 Pct Recovery = 95% Analysis Date = 09/05/13 Pct Recovery = 95% Analysis Date = 08/26/13 Pct Recovery = 96% Analysis Date = 08/26/13 Pct Recovery = 96% Analysis Date = 08/17/13 Pct Recovery = 96% Analysis Date = 08/17/13 Pct Recovery = 96% Analysis Date = 08/08/13 Pct Recovery = 96% Analysis Date = 08/08/13 Pct Recovery = 96% Analysis Date = 07/30/13 Pct Recovery = 97% Analysis Date = 07/30/13 Pct Recovery = 97% Analysis Date = 07/20/13 Pct Recovery = 97% Analysis Date = 07/20/13 Pct Recovery = 97% Analysis Date = 07/11/13 Pct Recovery = 98% Analysis Date = 07/11/13 Pct Recovery = 98% Analysis Date = 07/02/13 Pct Recovery = 98% Analysis Date = 07/02/13 Pct Recovery = 98% Analysis Date = 06/23/13 Pct Recovery = 99% Analysis Date = 06/23/13 Pct Recovery = 99% Analysis Date = 06/13/13 Pct Recovery = 99% Analysis Date = 06/13/13 Pct Recovery = 99% Analysis Date = 06/04/13 Pct Recovery = 100% Analysis Date = 06/04/13 Pct Recovery = 100% Analysis Date = 05/26/13 Pct Recovery = 100% Analysis Date = 05/26/13 Pct Recovery = 100% Analysis Date = 05/17/13 Pct Recovery = 101% Analysis Date = 05/17/13 Pct Recovery = 101% Analysis Date = 05/07/13 Pct Recovery = 101% Analysis Date = 05/07/13 Pct Recovery = 101% Analysis Date = 04/28/13 Pct Recovery = 102% Analysis Date = 04/28/13 Pct Recovery = 102% Analysis Date = 04/19/13 Pct Recovery = 102% Analysis Date = 04/19/13 Pct Recovery = 102% Analysis Date = 04/10/13 Pct Recovery = 103% Analysis Date = 04/10/13 Pct Recovery = 103% Analysis Date = 03/31/13 Pct Recovery = 103% Analysis Date = 03/31/13 Pct Recovery = 103% Analysis Date = 03/22/13 Pct Recovery = 104% Analysis Date = 03/22/13 Pct Recovery = 104% Analysis Date = 03/13/13 Pct Recovery = 104% Analysis Date = 03/13/13 Pct Recovery = 104% Analysis Date = 03/04/13 Pct Recovery = 105% Analysis Date = 03/04/13 Pct Recovery = 105% Analysis Date = 02/22/13 Pct Recovery = 105% Analysis Date = 02/22/13 Pct Recovery = 105% Analysis Date = 02/13/13 Pct Recovery = 105% Analysis Date = 02/13/13 Pct Recovery = 105% Analysis Date = 02/04/13 Pct Recovery = 106% Analysis Date = 02/04/13 Pct Recovery = 106% Analysis Date = 01/26/13 Pct Recovery = 106% Analysis Date = 01/26/13 Pct Recovery = 106% Analysis Date = 01/17/13 Pct Recovery = 107% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
CYANAZINE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 76 82% 23% 82% 19%
Total 76 82% 23% 82% 19%

Sample Statistics
CYANAZINE

Characteristic N % % Basis
Plotted 76 100% Spiked
Estimated Values 1 1% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 76 .  
False Negatives 0 0% 0 out of 76
Not Spiked 42 .  
False Positives 0 0% 0 out of 42

OBSP Determination:
CYFLUTHRIN
METHOD: 2033 , TESTIDCODE: 61585GCM39

Laboratory ID = 20140100085 Lab Value = 0.146 Expected Conc. = 0.186 Report level label = 0.016 Pct Recovery = 78% Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl SpecificMix = 042413 Laboratory ID = 20123560092 Lab Value = 0.017 Expected Conc. = 0.1265 Report level label = 0.016 Pct Recovery = 14% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = 0507-12-04.2 Laboratory ID = 20130810108 Lab Value = 0.096 Expected Conc. = 0.1252 Report level label = 0.016 Pct Recovery = 77% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl SpecificMix = LB92783 Laboratory ID = 20130100066 Lab Value = 0.082 Expected Conc. = 0.1252 Report level label = 0.016 Pct Recovery = 66% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl SpecificMix = LB92783 Laboratory ID = 20172510330 Lab Value = 0.051 Expected Conc. = 0.107 Report level label = 0.016 Pct Recovery = 47% Analysis Date = 12/29/17 SpikeMix = ChemService 6537100: 100 µl & Abs 071817Pest: 100 µl SpecificMix = 071817Pest Laboratory ID = 20163370001 Lab Value = 0.067 Expected Conc. = 0.1045 Report level label = 0.016 Pct Recovery = 64% Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl SpecificMix = LC20138V Laboratory ID = 20162860079 Lab Value = 0.062 Expected Conc. = 0.1 Report level label = 0.016 Pct Recovery = 62% Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl SpecificMix = 5054800 Laboratory ID = 20161880109 Lab Value = 0.089 Expected Conc. = 0.1 Report level label = 0.016 Pct Recovery = 89% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl SpecificMix = 5054800 Laboratory ID = 20152750006 Lab Value = 0.061 Expected Conc. = 0.096 Report level label = 0.016 Pct Recovery = 63% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl SpecificMix = EN150514012 Laboratory ID = 20152460215 Lab Value = 0.058 Expected Conc. = 0.096 Report level label = 0.016 Pct Recovery = 61% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl SpecificMix = EN150514012 Laboratory ID = 20132690010 Lab Value = 0.086 Expected Conc. = 0.093 Report level label = 0.016 Pct Recovery = 92% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl SpecificMix = 042413 Laboratory ID = 20132560001 Lab Value = 0.062 Expected Conc. = 0.093 Report level label = 0.016 Pct Recovery = 67% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl SpecificMix = 042413 Laboratory ID = 20132140002 Lab Value = 0.051 Expected Conc. = 0.091 Report level label = 0.016 Pct Recovery = 56% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl SpecificMix = 04CC101 Laboratory ID = 20171720140 Lab Value = 0.063 Expected Conc. = 0.0836 Report level label = 0.016 Pct Recovery = 76% Analysis Date = 08/31/17 SpikeMix = Supelco LC20138V: 80 µl & Phenova B20160331: 80 µl SpecificMix = LC20138V Laboratory ID = 20170740063 Lab Value = 0.058 Expected Conc. = 0.0836 Report level label = 0.016 Pct Recovery = 69% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl SpecificMix = LC20138V Laboratory ID = 20161470001 Lab Value = 0.075 Expected Conc. = 0.0836 Report level label = 0.016 Pct Recovery = 89% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl SpecificMix = LC20138V Laboratory ID = 20171380001 Lab Value = 0.051 Expected Conc. = 0.08 Report level label = 0.016 Pct Recovery = 63% Analysis Date = 06/07/17 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 5054800 Laboratory ID = 20170960001 Lab Value = 0.042 Expected Conc. = 0.08 Report level label = 0.016 Pct Recovery = 53% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl SpecificMix = 5054800 Laboratory ID = 20161740258 Lab Value = 0.050 Expected Conc. = 0.08 Report level label = 0.016 Pct Recovery = 63% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 5054800 Laboratory ID = 20150430092 Lab Value = 0.053 Expected Conc. = 0.066 Report level label = 0.016 Pct Recovery = 80% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl SpecificMix = E1140407002 Laboratory ID = 20143110108 Lab Value = 0.040 Expected Conc. = 0.066 Report level label = 0.016 Pct Recovery = 61% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl SpecificMix = E1140407002 Laboratory ID = 20142720002 Lab Value = 0.051 Expected Conc. = 0.066 Report level label = 0.016 Pct Recovery = 78% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl SpecificMix = E1140407002 Laboratory ID = 20141770149 Lab Value = 0.045 Expected Conc. = 0.066 Report level label = 0.016 Pct Recovery = 68% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl SpecificMix = E1140407002 Laboratory ID = 20143240095 Lab Value = 0.047 Expected Conc. = 0.0642 Report level label = 0.016 Pct Recovery = 73% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl SpecificMix = 032714 Laboratory ID = 20142270001 Lab Value = 0.051 Expected Conc. = 0.0642 Report level label = 0.016 Pct Recovery = 79% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl SpecificMix = 032714 Laboratory ID = 20141220025 Lab Value = 0.061 Expected Conc. = 0.0642 Report level label = 0.016 Pct Recovery = 94% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl SpecificMix = 032714 Laboratory ID = 20172560101 Lab Value = 0.052 Expected Conc. = 0.055 Report level label = 0.016 Pct Recovery = 94% Analysis Date = 12/22/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6567600: 50 µl SpecificMix = 6567600 Laboratory ID = 20130390105 Lab Value = 0.032 Expected Conc. = 0.0501 Report level label = 0.016 Pct Recovery = 64% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl SpecificMix = LB92783 Laboratory ID = 20160630046 Lab Value = 0.041 Expected Conc. = 0.048 Report level label = 0.016 Pct Recovery = 85% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = EN150514012 Laboratory ID = 20153440001 Lab Value = 0.030 Expected Conc. = 0.048 Report level label = 0.016 Pct Recovery = 63% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = EN150514012 Laboratory ID = 20171510080 Lab Value = 0.032 Expected Conc. = 0.0418 Report level label = 0.016 Pct Recovery = 76% Analysis Date = 06/09/17 SpikeMix = Supelco LC20138V: 40 µl & Crescent 03FF076: 40 µl SpecificMix = LC20138V Laboratory ID = 20162520001 Lab Value = 0.041 Expected Conc. = 0.0418 Report level label = 0.016 Pct Recovery = 98% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl SpecificMix = LC20138V Laboratory ID = 20162660005 Lab Value = 0.028 Expected Conc. = 0.0418 Report level label = 0.016 Pct Recovery = 67% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl SpecificMix = LC20138V Laboratory ID = 20162020124 Lab Value = 0.027 Expected Conc. = 0.0418 Report level label = 0.016 Pct Recovery = 64% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl SpecificMix = LC20138V Laboratory ID = 20171940002 Lab Value = 0.030 Expected Conc. = 0.04 Report level label = 0.016 Pct Recovery = 75% Analysis Date = 11/10/17 SpikeMix = ChemService 5054800: 40 µl & NSI 041816: 40 µl SpecificMix = 5054800 Laboratory ID = 20170460061 Lab Value = 0.023 Expected Conc. = 0.04 Report level label = 0.016 Pct Recovery = 58% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl SpecificMix = 5054800 Laboratory ID = 20163560019 Lab Value = 0.038 Expected Conc. = 0.04 Report level label = 0.016 Pct Recovery = 94% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl SpecificMix = 5054800 Laboratory ID = 20162150213 Lab Value = 0.044 Expected Conc. = 0.04 Report level label = 0.016 Pct Recovery = 109% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl SpecificMix = 5054800 Laboratory ID = 20133580036 Lab Value = 0.027 Expected Conc. = 0.0372 Report level label = 0.016 Pct Recovery = 73% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 042413 Laboratory ID = 20133190012 Lab Value = 0.050 Expected Conc. = 0.0372 Report level label = 0.016 Pct Recovery = 135% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 042413 Laboratory ID = 20131650073 Lab Value = 0.052 Expected Conc. = 0.0372 Report level label = 0.016 Pct Recovery = 139% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl SpecificMix = 042413 Laboratory ID = 20140730138 Lab Value = 0.024 Expected Conc. = 0.0364 Report level label = 0.016 Pct Recovery = 65% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 04CC101 Laboratory ID = 20140510043 Lab Value = 0.029 Expected Conc. = 0.0364 Report level label = 0.016 Pct Recovery = 79% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 04CC101 Laboratory ID = 20133310030 Lab Value = 0.043 Expected Conc. = 0.0364 Report level label = 0.016 Pct Recovery = 117% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl SpecificMix = 04CC101 Laboratory ID = 20132280016 Lab Value = 0.034 Expected Conc. = 0.0364 Report level label = 0.016 Pct Recovery = 92% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl SpecificMix = 04CC101 Laboratory ID = 20131510026 Lab Value = 0.035 Expected Conc. = 0.0364 Report level label = 0.016 Pct Recovery = 97% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl SpecificMix = 04CC101 Laboratory ID = 20142470041 Lab Value = 0.022 Expected Conc. = 0.033 Report level label = 0.016 Pct Recovery = 66% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141910243 Lab Value = 0.029 Expected Conc. = 0.033 Report level label = 0.016 Pct Recovery = 88% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141640076 Lab Value = 0.020 Expected Conc. = 0.033 Report level label = 0.016 Pct Recovery = 61% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141360094 Lab Value = 0.023 Expected Conc. = 0.033 Report level label = 0.016 Pct Recovery = 69% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = E1140407002 Laboratory ID = 20172780018 Lab Value = 0.027 Expected Conc. = 0.0321 Report level label = 0.016 Pct Recovery = 84% Analysis Date = 02/08/18 SpikeMix = ChemService 6537100: 30 µl & Abs 071817Pest: 30 µl SpecificMix = 071817Pest Laboratory ID = 20150150115 Lab Value = 0.034 Expected Conc. = 0.0321 Report level label = 0.016 Pct Recovery = 104% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl SpecificMix = 032714 Laboratory ID = 20142820151 Lab Value = 0.035 Expected Conc. = 0.0321 Report level label = 0.016 Pct Recovery = 109% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl SpecificMix = 032714 Laboratory ID = 20141490205 Lab Value = 0.024 Expected Conc. = 0.0321 Report level label = 0.016 Pct Recovery = 74% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = 032714 Laboratory ID = 20141080004 Lab Value = 0.022 Expected Conc. = 0.0321 Report level label = 0.016 Pct Recovery = 68% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl SpecificMix = 032714 Laboratory ID = 20160070059 Lab Value = 0.020 Expected Conc. = 0.024 Report level label = 0.016 Pct Recovery = 83% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = EN150514012 Laboratory ID = 20153160001 Lab Value = 0.020 Expected Conc. = 0.024 Report level label = 0.016 Pct Recovery = 83% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = EN150514012 Laboratory ID = 20151760208 Lab Value = 0.022 Expected Conc. = 0.024 Report level label = 0.016 Pct Recovery = 93% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl SpecificMix = EN150514012 Laboratory ID = 20151480170 Lab Value = 0.025 Expected Conc. = 0.024 Report level label = 0.016 Pct Recovery = 105% Analysis Date = 06/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150514012 Analysis Date = 02/08/18 Pct Recovery = 71% Analysis Date = 01/29/18 Pct Recovery = 71% Analysis Date = 01/29/18 Pct Recovery = 71% Analysis Date = 01/20/18 Pct Recovery = 71% Analysis Date = 01/20/18 Pct Recovery = 71% Analysis Date = 01/11/18 Pct Recovery = 72% Analysis Date = 01/11/18 Pct Recovery = 72% Analysis Date = 01/02/18 Pct Recovery = 72% Analysis Date = 01/02/18 Pct Recovery = 72% Analysis Date = 12/23/17 Pct Recovery = 72% Analysis Date = 12/23/17 Pct Recovery = 72% Analysis Date = 12/14/17 Pct Recovery = 72% Analysis Date = 12/14/17 Pct Recovery = 72% Analysis Date = 12/05/17 Pct Recovery = 72% Analysis Date = 12/05/17 Pct Recovery = 72% Analysis Date = 11/26/17 Pct Recovery = 72% Analysis Date = 11/26/17 Pct Recovery = 72% Analysis Date = 11/16/17 Pct Recovery = 72% Analysis Date = 11/16/17 Pct Recovery = 72% Analysis Date = 11/07/17 Pct Recovery = 72% Analysis Date = 11/07/17 Pct Recovery = 72% Analysis Date = 10/29/17 Pct Recovery = 72% Analysis Date = 10/29/17 Pct Recovery = 72% Analysis Date = 10/20/17 Pct Recovery = 72% Analysis Date = 10/20/17 Pct Recovery = 72% Analysis Date = 10/10/17 Pct Recovery = 72% Analysis Date = 10/10/17 Pct Recovery = 72% Analysis Date = 10/01/17 Pct Recovery = 73% Analysis Date = 10/01/17 Pct Recovery = 73% Analysis Date = 09/22/17 Pct Recovery = 73% Analysis Date = 09/22/17 Pct Recovery = 73% Analysis Date = 09/13/17 Pct Recovery = 73% Analysis Date = 09/13/17 Pct Recovery = 73% Analysis Date = 09/03/17 Pct Recovery = 73% Analysis Date = 09/03/17 Pct Recovery = 73% Analysis Date = 08/25/17 Pct Recovery = 73% Analysis Date = 08/25/17 Pct Recovery = 73% Analysis Date = 08/16/17 Pct Recovery = 73% Analysis Date = 08/16/17 Pct Recovery = 73% Analysis Date = 08/07/17 Pct Recovery = 73% Analysis Date = 08/07/17 Pct Recovery = 73% Analysis Date = 07/28/17 Pct Recovery = 73% Analysis Date = 07/28/17 Pct Recovery = 73% Analysis Date = 07/19/17 Pct Recovery = 73% Analysis Date = 07/19/17 Pct Recovery = 73% Analysis Date = 07/10/17 Pct Recovery = 73% Analysis Date = 07/10/17 Pct Recovery = 73% Analysis Date = 07/01/17 Pct Recovery = 73% Analysis Date = 07/01/17 Pct Recovery = 73% Analysis Date = 06/21/17 Pct Recovery = 73% Analysis Date = 06/21/17 Pct Recovery = 73% Analysis Date = 06/12/17 Pct Recovery = 74% Analysis Date = 06/12/17 Pct Recovery = 74% Analysis Date = 06/03/17 Pct Recovery = 74% Analysis Date = 06/03/17 Pct Recovery = 74% Analysis Date = 05/25/17 Pct Recovery = 74% Analysis Date = 05/25/17 Pct Recovery = 74% Analysis Date = 05/15/17 Pct Recovery = 74% Analysis Date = 05/15/17 Pct Recovery = 74% Analysis Date = 05/06/17 Pct Recovery = 74% Analysis Date = 05/06/17 Pct Recovery = 74% Analysis Date = 04/27/17 Pct Recovery = 74% Analysis Date = 04/27/17 Pct Recovery = 74% Analysis Date = 04/18/17 Pct Recovery = 74% Analysis Date = 04/18/17 Pct Recovery = 74% Analysis Date = 04/08/17 Pct Recovery = 74% Analysis Date = 04/08/17 Pct Recovery = 74% Analysis Date = 03/30/17 Pct Recovery = 74% Analysis Date = 03/30/17 Pct Recovery = 74% Analysis Date = 03/21/17 Pct Recovery = 74% Analysis Date = 03/21/17 Pct Recovery = 74% Analysis Date = 03/12/17 Pct Recovery = 74% Analysis Date = 03/12/17 Pct Recovery = 74% Analysis Date = 03/02/17 Pct Recovery = 74% Analysis Date = 03/02/17 Pct Recovery = 74% Analysis Date = 02/21/17 Pct Recovery = 75% Analysis Date = 02/21/17 Pct Recovery = 75% Analysis Date = 02/12/17 Pct Recovery = 75% Analysis Date = 02/12/17 Pct Recovery = 75% Analysis Date = 02/03/17 Pct Recovery = 75% Analysis Date = 02/03/17 Pct Recovery = 75% Analysis Date = 01/24/17 Pct Recovery = 75% Analysis Date = 01/24/17 Pct Recovery = 75% Analysis Date = 01/15/17 Pct Recovery = 75% Analysis Date = 01/15/17 Pct Recovery = 75% Analysis Date = 01/06/17 Pct Recovery = 75% Analysis Date = 01/06/17 Pct Recovery = 75% Analysis Date = 12/28/16 Pct Recovery = 75% Analysis Date = 12/28/16 Pct Recovery = 75% Analysis Date = 12/18/16 Pct Recovery = 75% Analysis Date = 12/18/16 Pct Recovery = 75% Analysis Date = 12/09/16 Pct Recovery = 75% Analysis Date = 12/09/16 Pct Recovery = 75% Analysis Date = 11/30/16 Pct Recovery = 76% Analysis Date = 11/30/16 Pct Recovery = 76% Analysis Date = 11/21/16 Pct Recovery = 76% Analysis Date = 11/21/16 Pct Recovery = 76% Analysis Date = 11/11/16 Pct Recovery = 76% Analysis Date = 11/11/16 Pct Recovery = 76% Analysis Date = 11/02/16 Pct Recovery = 76% Analysis Date = 11/02/16 Pct Recovery = 76% Analysis Date = 10/24/16 Pct Recovery = 76% Analysis Date = 10/24/16 Pct Recovery = 76% Analysis Date = 10/15/16 Pct Recovery = 76% Analysis Date = 10/15/16 Pct Recovery = 76% Analysis Date = 10/05/16 Pct Recovery = 76% Analysis Date = 10/05/16 Pct Recovery = 76% Analysis Date = 09/26/16 Pct Recovery = 77% Analysis Date = 09/26/16 Pct Recovery = 77% Analysis Date = 09/17/16 Pct Recovery = 77% Analysis Date = 09/17/16 Pct Recovery = 77% Analysis Date = 09/08/16 Pct Recovery = 77% Analysis Date = 09/08/16 Pct Recovery = 77% Analysis Date = 08/29/16 Pct Recovery = 77% Analysis Date = 08/29/16 Pct Recovery = 77% Analysis Date = 08/20/16 Pct Recovery = 77% Analysis Date = 08/20/16 Pct Recovery = 77% Analysis Date = 08/11/16 Pct Recovery = 77% Analysis Date = 08/11/16 Pct Recovery = 77% Analysis Date = 08/02/16 Pct Recovery = 77% Analysis Date = 08/02/16 Pct Recovery = 77% Analysis Date = 07/23/16 Pct Recovery = 77% Analysis Date = 07/23/16 Pct Recovery = 77% Analysis Date = 07/14/16 Pct Recovery = 78% Analysis Date = 07/14/16 Pct Recovery = 78% Analysis Date = 07/05/16 Pct Recovery = 78% Analysis Date = 07/05/16 Pct Recovery = 78% Analysis Date = 06/26/16 Pct Recovery = 78% Analysis Date = 06/26/16 Pct Recovery = 78% Analysis Date = 06/16/16 Pct Recovery = 78% Analysis Date = 06/16/16 Pct Recovery = 78% Analysis Date = 06/07/16 Pct Recovery = 78% Analysis Date = 06/07/16 Pct Recovery = 78% Analysis Date = 05/29/16 Pct Recovery = 78% Analysis Date = 05/29/16 Pct Recovery = 78% Analysis Date = 05/20/16 Pct Recovery = 78% Analysis Date = 05/20/16 Pct Recovery = 78% Analysis Date = 05/10/16 Pct Recovery = 78% Analysis Date = 05/10/16 Pct Recovery = 78% Analysis Date = 05/01/16 Pct Recovery = 79% Analysis Date = 05/01/16 Pct Recovery = 79% Analysis Date = 04/22/16 Pct Recovery = 79% Analysis Date = 04/22/16 Pct Recovery = 79% Analysis Date = 04/13/16 Pct Recovery = 79% Analysis Date = 04/13/16 Pct Recovery = 79% Analysis Date = 04/03/16 Pct Recovery = 79% Analysis Date = 04/03/16 Pct Recovery = 79% Analysis Date = 03/25/16 Pct Recovery = 79% Analysis Date = 03/25/16 Pct Recovery = 79% Analysis Date = 03/16/16 Pct Recovery = 79% Analysis Date = 03/16/16 Pct Recovery = 79% Analysis Date = 03/07/16 Pct Recovery = 79% Analysis Date = 03/07/16 Pct Recovery = 79% Analysis Date = 02/26/16 Pct Recovery = 80% Analysis Date = 02/26/16 Pct Recovery = 80% Analysis Date = 02/17/16 Pct Recovery = 80% Analysis Date = 02/17/16 Pct Recovery = 80% Analysis Date = 02/08/16 Pct Recovery = 80% Analysis Date = 02/08/16 Pct Recovery = 80% Analysis Date = 01/30/16 Pct Recovery = 80% Analysis Date = 01/30/16 Pct Recovery = 80% Analysis Date = 01/20/16 Pct Recovery = 80% Analysis Date = 01/20/16 Pct Recovery = 80% Analysis Date = 01/11/16 Pct Recovery = 80% Analysis Date = 01/11/16 Pct Recovery = 80% Analysis Date = 01/02/16 Pct Recovery = 80% Analysis Date = 01/02/16 Pct Recovery = 80% Analysis Date = 12/24/15 Pct Recovery = 80% Analysis Date = 12/24/15 Pct Recovery = 80% Analysis Date = 12/14/15 Pct Recovery = 80% Analysis Date = 12/14/15 Pct Recovery = 80% Analysis Date = 12/05/15 Pct Recovery = 80% Analysis Date = 12/05/15 Pct Recovery = 80% Analysis Date = 11/26/15 Pct Recovery = 80% Analysis Date = 11/26/15 Pct Recovery = 80% Analysis Date = 11/17/15 Pct Recovery = 80% Analysis Date = 11/17/15 Pct Recovery = 80% Analysis Date = 11/07/15 Pct Recovery = 80% Analysis Date = 11/07/15 Pct Recovery = 80% Analysis Date = 10/29/15 Pct Recovery = 80% Analysis Date = 10/29/15 Pct Recovery = 80% Analysis Date = 10/20/15 Pct Recovery = 80% Analysis Date = 10/20/15 Pct Recovery = 80% Analysis Date = 10/11/15 Pct Recovery = 80% Analysis Date = 10/11/15 Pct Recovery = 80% Analysis Date = 10/01/15 Pct Recovery = 80% Analysis Date = 10/01/15 Pct Recovery = 80% Analysis Date = 09/22/15 Pct Recovery = 80% Analysis Date = 09/22/15 Pct Recovery = 80% Analysis Date = 09/13/15 Pct Recovery = 80% Analysis Date = 09/13/15 Pct Recovery = 80% Analysis Date = 09/04/15 Pct Recovery = 80% Analysis Date = 09/04/15 Pct Recovery = 80% Analysis Date = 08/25/15 Pct Recovery = 80% Analysis Date = 08/25/15 Pct Recovery = 80% Analysis Date = 08/16/15 Pct Recovery = 80% Analysis Date = 08/16/15 Pct Recovery = 80% Analysis Date = 08/07/15 Pct Recovery = 80% Analysis Date = 08/07/15 Pct Recovery = 80% Analysis Date = 07/29/15 Pct Recovery = 80% Analysis Date = 07/29/15 Pct Recovery = 80% Analysis Date = 07/19/15 Pct Recovery = 80% Analysis Date = 07/19/15 Pct Recovery = 80% Analysis Date = 07/10/15 Pct Recovery = 80% Analysis Date = 07/10/15 Pct Recovery = 80% Analysis Date = 07/01/15 Pct Recovery = 80% Analysis Date = 07/01/15 Pct Recovery = 80% Analysis Date = 06/22/15 Pct Recovery = 80% Analysis Date = 06/22/15 Pct Recovery = 80% Analysis Date = 06/12/15 Pct Recovery = 80% Analysis Date = 06/12/15 Pct Recovery = 80% Analysis Date = 06/03/15 Pct Recovery = 80% Analysis Date = 06/03/15 Pct Recovery = 80% Analysis Date = 05/25/15 Pct Recovery = 80% Analysis Date = 05/25/15 Pct Recovery = 80% Analysis Date = 05/16/15 Pct Recovery = 80% Analysis Date = 05/16/15 Pct Recovery = 80% Analysis Date = 05/06/15 Pct Recovery = 80% Analysis Date = 05/06/15 Pct Recovery = 80% Analysis Date = 04/27/15 Pct Recovery = 80% Analysis Date = 04/27/15 Pct Recovery = 80% Analysis Date = 04/18/15 Pct Recovery = 80% Analysis Date = 04/18/15 Pct Recovery = 80% Analysis Date = 04/09/15 Pct Recovery = 80% Analysis Date = 04/09/15 Pct Recovery = 80% Analysis Date = 03/30/15 Pct Recovery = 80% Analysis Date = 03/30/15 Pct Recovery = 80% Analysis Date = 03/21/15 Pct Recovery = 80% Analysis Date = 03/21/15 Pct Recovery = 80% Analysis Date = 03/12/15 Pct Recovery = 80% Analysis Date = 03/12/15 Pct Recovery = 80% Analysis Date = 03/03/15 Pct Recovery = 80% Analysis Date = 03/03/15 Pct Recovery = 80% Analysis Date = 02/21/15 Pct Recovery = 80% Analysis Date = 02/21/15 Pct Recovery = 80% Analysis Date = 02/12/15 Pct Recovery = 80% Analysis Date = 02/12/15 Pct Recovery = 80% Analysis Date = 02/03/15 Pct Recovery = 80% Analysis Date = 02/03/15 Pct Recovery = 80% Analysis Date = 01/25/15 Pct Recovery = 80% Analysis Date = 01/25/15 Pct Recovery = 80% Analysis Date = 01/15/15 Pct Recovery = 80% Analysis Date = 01/15/15 Pct Recovery = 80% Analysis Date = 01/06/15 Pct Recovery = 80% Analysis Date = 01/06/15 Pct Recovery = 80% Analysis Date = 12/28/14 Pct Recovery = 80% Analysis Date = 12/28/14 Pct Recovery = 80% Analysis Date = 12/19/14 Pct Recovery = 80% Analysis Date = 12/19/14 Pct Recovery = 80% Analysis Date = 12/09/14 Pct Recovery = 80% Analysis Date = 12/09/14 Pct Recovery = 80% Analysis Date = 11/30/14 Pct Recovery = 80% Analysis Date = 11/30/14 Pct Recovery = 80% Analysis Date = 11/21/14 Pct Recovery = 80% Analysis Date = 11/21/14 Pct Recovery = 80% Analysis Date = 11/12/14 Pct Recovery = 81% Analysis Date = 11/12/14 Pct Recovery = 81% Analysis Date = 11/02/14 Pct Recovery = 81% Analysis Date = 11/02/14 Pct Recovery = 81% Analysis Date = 10/24/14 Pct Recovery = 81% Analysis Date = 10/24/14 Pct Recovery = 81% Analysis Date = 10/15/14 Pct Recovery = 81% Analysis Date = 10/15/14 Pct Recovery = 81% Analysis Date = 10/06/14 Pct Recovery = 81% Analysis Date = 10/06/14 Pct Recovery = 81% Analysis Date = 09/26/14 Pct Recovery = 81% Analysis Date = 09/26/14 Pct Recovery = 81% Analysis Date = 09/17/14 Pct Recovery = 81% Analysis Date = 09/17/14 Pct Recovery = 81% Analysis Date = 09/08/14 Pct Recovery = 81% Analysis Date = 09/08/14 Pct Recovery = 81% Analysis Date = 08/30/14 Pct Recovery = 81% Analysis Date = 08/30/14 Pct Recovery = 81% Analysis Date = 08/20/14 Pct Recovery = 81% Analysis Date = 08/20/14 Pct Recovery = 81% Analysis Date = 08/11/14 Pct Recovery = 81% Analysis Date = 08/11/14 Pct Recovery = 81% Analysis Date = 08/02/14 Pct Recovery = 81% Analysis Date = 08/02/14 Pct Recovery = 81% Analysis Date = 07/24/14 Pct Recovery = 82% Analysis Date = 07/24/14 Pct Recovery = 82% Analysis Date = 07/14/14 Pct Recovery = 82% Analysis Date = 07/14/14 Pct Recovery = 82% Analysis Date = 07/05/14 Pct Recovery = 82% Analysis Date = 07/05/14 Pct Recovery = 82% Analysis Date = 06/26/14 Pct Recovery = 82% Analysis Date = 06/26/14 Pct Recovery = 82% Analysis Date = 06/17/14 Pct Recovery = 82% Analysis Date = 06/17/14 Pct Recovery = 82% Analysis Date = 06/07/14 Pct Recovery = 82% Analysis Date = 06/07/14 Pct Recovery = 82% Analysis Date = 05/29/14 Pct Recovery = 82% Analysis Date = 05/29/14 Pct Recovery = 82% Analysis Date = 05/20/14 Pct Recovery = 82% Analysis Date = 05/20/14 Pct Recovery = 82% Analysis Date = 05/11/14 Pct Recovery = 82% Analysis Date = 05/11/14 Pct Recovery = 82% Analysis Date = 05/01/14 Pct Recovery = 82% Analysis Date = 05/01/14 Pct Recovery = 82% Analysis Date = 04/22/14 Pct Recovery = 82% Analysis Date = 04/22/14 Pct Recovery = 82% Analysis Date = 04/13/14 Pct Recovery = 82% Analysis Date = 04/13/14 Pct Recovery = 82% Analysis Date = 04/04/14 Pct Recovery = 82% Analysis Date = 04/04/14 Pct Recovery = 82% Analysis Date = 03/25/14 Pct Recovery = 82% Analysis Date = 03/25/14 Pct Recovery = 82% Analysis Date = 03/16/14 Pct Recovery = 82% Analysis Date = 03/16/14 Pct Recovery = 82% Analysis Date = 03/07/14 Pct Recovery = 82% Analysis Date = 03/07/14 Pct Recovery = 82% Analysis Date = 02/26/14 Pct Recovery = 82% Analysis Date = 02/26/14 Pct Recovery = 82% Analysis Date = 02/16/14 Pct Recovery = 81% Analysis Date = 02/16/14 Pct Recovery = 81% Analysis Date = 02/07/14 Pct Recovery = 81% Analysis Date = 02/07/14 Pct Recovery = 81% Analysis Date = 01/29/14 Pct Recovery = 81% Analysis Date = 01/29/14 Pct Recovery = 81% Analysis Date = 01/20/14 Pct Recovery = 81% Analysis Date = 01/20/14 Pct Recovery = 81% Analysis Date = 01/10/14 Pct Recovery = 81% Analysis Date = 01/10/14 Pct Recovery = 81% Analysis Date = 01/01/14 Pct Recovery = 81% Analysis Date = 01/01/14 Pct Recovery = 81% Analysis Date = 12/23/13 Pct Recovery = 80% Analysis Date = 12/23/13 Pct Recovery = 80% Analysis Date = 12/14/13 Pct Recovery = 80% Analysis Date = 12/14/13 Pct Recovery = 80% Analysis Date = 12/04/13 Pct Recovery = 80% Analysis Date = 12/04/13 Pct Recovery = 80% Analysis Date = 11/25/13 Pct Recovery = 80% Analysis Date = 11/25/13 Pct Recovery = 80% Analysis Date = 11/16/13 Pct Recovery = 80% Analysis Date = 11/16/13 Pct Recovery = 80% Analysis Date = 11/07/13 Pct Recovery = 80% Analysis Date = 11/07/13 Pct Recovery = 80% Analysis Date = 10/28/13 Pct Recovery = 80% Analysis Date = 10/28/13 Pct Recovery = 80% Analysis Date = 10/19/13 Pct Recovery = 79% Analysis Date = 10/19/13 Pct Recovery = 79% Analysis Date = 10/10/13 Pct Recovery = 79% Analysis Date = 10/10/13 Pct Recovery = 79% Analysis Date = 10/01/13 Pct Recovery = 79% Analysis Date = 10/01/13 Pct Recovery = 79% Analysis Date = 09/21/13 Pct Recovery = 79% Analysis Date = 09/21/13 Pct Recovery = 79% Analysis Date = 09/12/13 Pct Recovery = 79% Analysis Date = 09/12/13 Pct Recovery = 79% Analysis Date = 09/03/13 Pct Recovery = 79% Analysis Date = 09/03/13 Pct Recovery = 79% Analysis Date = 08/25/13 Pct Recovery = 79% Analysis Date = 08/25/13 Pct Recovery = 79% Analysis Date = 08/15/13 Pct Recovery = 78% Analysis Date = 08/15/13 Pct Recovery = 78% Analysis Date = 08/06/13 Pct Recovery = 78% Analysis Date = 08/06/13 Pct Recovery = 78% Analysis Date = 07/28/13 Pct Recovery = 78% Analysis Date = 07/28/13 Pct Recovery = 78% Analysis Date = 07/19/13 Pct Recovery = 78% Analysis Date = 07/19/13 Pct Recovery = 78% Analysis Date = 07/09/13 Pct Recovery = 78% Analysis Date = 07/09/13 Pct Recovery = 78% Analysis Date = 06/30/13 Pct Recovery = 78% Analysis Date = 06/30/13 Pct Recovery = 78% Analysis Date = 06/21/13 Pct Recovery = 78% Analysis Date = 06/21/13 Pct Recovery = 78% Analysis Date = 06/12/13 Pct Recovery = 77% Analysis Date = 06/12/13 Pct Recovery = 77% Analysis Date = 06/02/13 Pct Recovery = 77% Analysis Date = 06/02/13 Pct Recovery = 77% Analysis Date = 05/24/13 Pct Recovery = 77% Analysis Date = 05/24/13 Pct Recovery = 77% Analysis Date = 05/15/13 Pct Recovery = 77% Analysis Date = 05/15/13 Pct Recovery = 77% Analysis Date = 05/06/13 Pct Recovery = 77% Analysis Date = 05/06/13 Pct Recovery = 77% Analysis Date = 04/26/13 Pct Recovery = 77% Analysis Date = 04/26/13 Pct Recovery = 77% Analysis Date = 04/17/13 Pct Recovery = 77% Analysis Date = 04/17/13 Pct Recovery = 77% Analysis Date = 04/08/13 Pct Recovery = 76% Analysis Date = 04/08/13 Pct Recovery = 76% Analysis Date = 03/30/13 Pct Recovery = 76% Analysis Date = 03/30/13 Pct Recovery = 76% Analysis Date = 03/20/13 Pct Recovery = 76% Analysis Date = 03/20/13 Pct Recovery = 76% Analysis Date = 03/11/13 Pct Recovery = 76% Analysis Date = 03/11/13 Pct Recovery = 76% Analysis Date = 03/02/13 Pct Recovery = 76% Analysis Date = 03/02/13 Pct Recovery = 76% Analysis Date = 02/21/13 Pct Recovery = 76% Analysis Date = 02/21/13 Pct Recovery = 76% Analysis Date = 02/11/13 Pct Recovery = 75% Analysis Date = 02/11/13 Pct Recovery = 75% Analysis Date = 02/02/13 Pct Recovery = 75% Analysis Date = 02/02/13 Pct Recovery = 75% Analysis Date = 01/24/13 Pct Recovery = 75% Analysis Date = 01/24/13 Pct Recovery = 75% Analysis Date = 01/15/13 Pct Recovery = 75% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
CYFLUTHRIN

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 59 78% 21% 76% 21%
Total 59 78% 21% 76% 21%

Sample Statistics
CYFLUTHRIN

Characteristic N % % Basis
Plotted 59 97% Spiked
Estimated Values 59 97% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 61 .  
False Negatives 2 3% 2 out of 61
Not Spiked 48 .  
False Positives 0 0% 0 out of 48

OBSP Determination:
CYHALOTHRIN
METHOD: 2033 , TESTIDCODE: 61595GCM39

Laboratory ID = 20132490342 Lab Value = 0.082 Expected Conc. = 0.22 Report level label = 0.014 Pct Recovery = 37% Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20132140002 Lab Value = 0.058 Expected Conc. = 0.1132 Report level label = 0.014 Pct Recovery = 51% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl SpecificMix = LB99392 Laboratory ID = 20131370001 Lab Value = 0.091 Expected Conc. = 0.1132 Report level label = 0.014 Pct Recovery = 80% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl SpecificMix = LB99392 Laboratory ID = 20140370077 Lab Value = 0.044 Expected Conc. = 0.11 Report level label = 0.014 Pct Recovery = 40% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20132560001 Lab Value = 0.051 Expected Conc. = 0.11 Report level label = 0.014 Pct Recovery = 47% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20130250061 Lab Value = 0.051 Expected Conc. = 0.1 Report level label = 0.014 Pct Recovery = 51% Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl SpecificMix = A088380 Laboratory ID = 20172510330 Lab Value = 0.046 Expected Conc. = 0.093 Report level label = 0.014 Pct Recovery = 50% Analysis Date = 12/29/17 SpikeMix = ChemService 6537100: 100 µl & Abs 071817Pest: 100 µl SpecificMix = 071817Pest Laboratory ID = 20162860079 Lab Value = 0.051 Expected Conc. = 0.088 Report level label = 0.014 Pct Recovery = 58% Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl SpecificMix = 060916 Laboratory ID = 20163150006 Lab Value = 0.057 Expected Conc. = 0.088 Report level label = 0.014 Pct Recovery = 64% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl SpecificMix = 060916 Laboratory ID = 20152750006 Lab Value = 0.044 Expected Conc. = 0.084 Report level label = 0.014 Pct Recovery = 53% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl SpecificMix = EN150514012 Laboratory ID = 20152460215 Lab Value = 0.033 Expected Conc. = 0.084 Report level label = 0.014 Pct Recovery = 40% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl SpecificMix = EN150514012 Laboratory ID = 20171660002 Lab Value = 0.040 Expected Conc. = 0.0704 Report level label = 0.014 Pct Recovery = 57% Analysis Date = 08/23/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = 060916 Laboratory ID = 20171380001 Lab Value = 0.049 Expected Conc. = 0.0704 Report level label = 0.014 Pct Recovery = 69% Analysis Date = 06/07/17 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 041816 Laboratory ID = 20170740063 Lab Value = 0.051 Expected Conc. = 0.0704 Report level label = 0.014 Pct Recovery = 73% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl SpecificMix = 041816 Laboratory ID = 20170190026 Lab Value = 0.036 Expected Conc. = 0.0704 Report level label = 0.014 Pct Recovery = 51% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = 060916 Laboratory ID = 20161740258 Lab Value = 0.043 Expected Conc. = 0.0704 Report level label = 0.014 Pct Recovery = 61% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 041816 Laboratory ID = 20150430092 Lab Value = 0.040 Expected Conc. = 0.0559 Report level label = 0.014 Pct Recovery = 71% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl SpecificMix = E1140407002 Laboratory ID = 20143110108 Lab Value = 0.030 Expected Conc. = 0.0559 Report level label = 0.014 Pct Recovery = 54% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl SpecificMix = E1140407002 Laboratory ID = 20142720002 Lab Value = 0.031 Expected Conc. = 0.0559 Report level label = 0.014 Pct Recovery = 55% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl SpecificMix = E1140407002 Laboratory ID = 20141770149 Lab Value = 0.029 Expected Conc. = 0.0559 Report level label = 0.014 Pct Recovery = 53% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl SpecificMix = E1140407002 Laboratory ID = 20143240095 Lab Value = 0.036 Expected Conc. = 0.0558 Report level label = 0.014 Pct Recovery = 65% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl SpecificMix = 032714 Laboratory ID = 20142270001 Lab Value = 0.033 Expected Conc. = 0.0558 Report level label = 0.014 Pct Recovery = 58% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl SpecificMix = 032714 Laboratory ID = 20141220025 Lab Value = 0.036 Expected Conc. = 0.0558 Report level label = 0.014 Pct Recovery = 65% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl SpecificMix = 032714 Laboratory ID = 20140230082 Lab Value = 0.033 Expected Conc. = 0.05 Report level label = 0.014 Pct Recovery = 67% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl SpecificMix = A093651 Laboratory ID = 20132420001 Lab Value = 0.026 Expected Conc. = 0.05 Report level label = 0.014 Pct Recovery = 53% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl SpecificMix = A093651 Laboratory ID = 20130810108 Lab Value = 0.032 Expected Conc. = 0.05 Report level label = 0.014 Pct Recovery = 64% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl SpecificMix = T1120530013 Laboratory ID = 20123560092 Lab Value = 0.020 Expected Conc. = 0.05 Report level label = 0.014 Pct Recovery = 40% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = T1120530013 Laboratory ID = 20140510043 Lab Value = 0.032 Expected Conc. = 0.0453 Report level label = 0.014 Pct Recovery = 70% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl SpecificMix = LB99392 Laboratory ID = 20133470008 Lab Value = 0.025 Expected Conc. = 0.0453 Report level label = 0.014 Pct Recovery = 55% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl SpecificMix = LB99392 Laboratory ID = 20133190012 Lab Value = 0.031 Expected Conc. = 0.0453 Report level label = 0.014 Pct Recovery = 69% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = LB99392 Laboratory ID = 20133050050 Lab Value = 0.029 Expected Conc. = 0.0453 Report level label = 0.014 Pct Recovery = 64% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl SpecificMix = LB99392 Laboratory ID = 20172560101 Lab Value = 0.046 Expected Conc. = 0.045 Report level label = 0.014 Pct Recovery = 103% Analysis Date = 12/22/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6567600: 50 µl SpecificMix = 6567600 Laboratory ID = 20133580036 Lab Value = 0.021 Expected Conc. = 0.044 Report level label = 0.014 Pct Recovery = 48% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20131790009 Lab Value = 0.015 Expected Conc. = 0.044 Report level label = 0.014 Pct Recovery = 35% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20131510026 Lab Value = 0.032 Expected Conc. = 0.044 Report level label = 0.014 Pct Recovery = 73% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20160630046 Lab Value = 0.030 Expected Conc. = 0.042 Report level label = 0.014 Pct Recovery = 71% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = EN150514012 Laboratory ID = 20153440001 Lab Value = 0.022 Expected Conc. = 0.042 Report level label = 0.014 Pct Recovery = 51% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = EN150514012 Laboratory ID = 20152330039 Lab Value = 0.024 Expected Conc. = 0.042 Report level label = 0.014 Pct Recovery = 56% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl SpecificMix = 041415 Laboratory ID = 20151900132 Lab Value = 0.044 Expected Conc. = 0.042 Report level label = 0.014 Pct Recovery = 104% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl SpecificMix = 041415 Laboratory ID = 20151270112 Lab Value = 0.030 Expected Conc. = 0.042 Report level label = 0.014 Pct Recovery = 71% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl SpecificMix = 041415 Laboratory ID = 20171940002 Lab Value = 0.032 Expected Conc. = 0.0352 Report level label = 0.014 Pct Recovery = 90% Analysis Date = 11/10/17 SpikeMix = ChemService 5054800: 40 µl & NSI 041816: 40 µl SpecificMix = 041816 Laboratory ID = 20171160110 Lab Value = 0.023 Expected Conc. = 0.0352 Report level label = 0.014 Pct Recovery = 65% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = 060916 Laboratory ID = 20162520001 Lab Value = 0.028 Expected Conc. = 0.0352 Report level label = 0.014 Pct Recovery = 79% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl SpecificMix = 060916 Laboratory ID = 20163560019 Lab Value = 0.029 Expected Conc. = 0.0352 Report level label = 0.014 Pct Recovery = 83% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl SpecificMix = 060916 Laboratory ID = 20162380004 Lab Value = 0.020 Expected Conc. = 0.0352 Report level label = 0.014 Pct Recovery = 57% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = 060916 Laboratory ID = 20162020124 Lab Value = 0.024 Expected Conc. = 0.0352 Report level label = 0.014 Pct Recovery = 69% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl SpecificMix = 041816 Laboratory ID = 20161600087 Lab Value = 0.029 Expected Conc. = 0.0352 Report level label = 0.014 Pct Recovery = 83% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 041816 Laboratory ID = 20161340228 Lab Value = 0.030 Expected Conc. = 0.0352 Report level label = 0.014 Pct Recovery = 84% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl SpecificMix = 041816 Laboratory ID = 20161190075 Lab Value = 0.032 Expected Conc. = 0.0352 Report level label = 0.014 Pct Recovery = 89% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 041816 Laboratory ID = 20142470041 Lab Value = 0.014 Expected Conc. = 0.028 Report level label = 0.014 Pct Recovery = 50% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141910243 Lab Value = 0.015 Expected Conc. = 0.028 Report level label = 0.014 Pct Recovery = 54% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141640076 Lab Value = 0.011 Expected Conc. = 0.028 Report level label = 0.014 Pct Recovery = 38% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141360094 Lab Value = 0.014 Expected Conc. = 0.028 Report level label = 0.014 Pct Recovery = 48% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = E1140407002 Laboratory ID = 20172780018 Lab Value = 0.027 Expected Conc. = 0.0279 Report level label = 0.014 Pct Recovery = 97% Analysis Date = 02/08/18 SpikeMix = ChemService 6537100: 30 µl & Abs 071817Pest: 30 µl SpecificMix = 071817Pest Laboratory ID = 20150150115 Lab Value = 0.025 Expected Conc. = 0.0279 Report level label = 0.014 Pct Recovery = 89% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl SpecificMix = 032714 Laboratory ID = 20142820151 Lab Value = 0.024 Expected Conc. = 0.0279 Report level label = 0.014 Pct Recovery = 87% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl SpecificMix = 032714 Laboratory ID = 20141490205 Lab Value = 0.016 Expected Conc. = 0.0279 Report level label = 0.014 Pct Recovery = 57% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = 032714 Laboratory ID = 20141080004 Lab Value = 0.016 Expected Conc. = 0.0279 Report level label = 0.014 Pct Recovery = 57% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl SpecificMix = 032714 Laboratory ID = 20161050143 Lab Value = 0.015 Expected Conc. = 0.021 Report level label = 0.014 Pct Recovery = 70% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 041415 Laboratory ID = 20160210080 Lab Value = 0.014 Expected Conc. = 0.021 Report level label = 0.014 Pct Recovery = 65% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 041415 Laboratory ID = 20160070059 Lab Value = 0.013 Expected Conc. = 0.021 Report level label = 0.014 Pct Recovery = 60% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = EN150514012 Laboratory ID = 20153160001 Lab Value = 0.012 Expected Conc. = 0.021 Report level label = 0.014 Pct Recovery = 55% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = EN150514012 Laboratory ID = 20152950078 Lab Value = 0.011 Expected Conc. = 0.021 Report level label = 0.014 Pct Recovery = 51% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 041415 Laboratory ID = 20152040177 Lab Value = 0.019 Expected Conc. = 0.021 Report level label = 0.014 Pct Recovery = 90% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl SpecificMix = 041415 Laboratory ID = 20151760208 Lab Value = 0.013 Expected Conc. = 0.021 Report level label = 0.014 Pct Recovery = 62% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl SpecificMix = EN150514012 Laboratory ID = 20151480170 Lab Value = 0.014 Expected Conc. = 0.021 Report level label = 0.014 Pct Recovery = 66% Analysis Date = 06/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150514012 Laboratory ID = 20151210037 Lab Value = 0.014 Expected Conc. = 0.021 Report level label = 0.014 Pct Recovery = 68% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 041415 Laboratory ID = 20140860102 Lab Value = 0.011 Expected Conc. = 0.02 Report level label = 0.014 Pct Recovery = 55% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl SpecificMix = A093651 Laboratory ID = 20133400002 Lab Value = 0.011 Expected Conc. = 0.02 Report level label = 0.014 Pct Recovery = 57% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = A093651 Laboratory ID = 20132910008 Lab Value = 0.012 Expected Conc. = 0.02 Report level label = 0.014 Pct Recovery = 58% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = A093651 Laboratory ID = 20131920149 Lab Value = 0.010 Expected Conc. = 0.02 Report level label = 0.014 Pct Recovery = 49% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl SpecificMix = A093651 Laboratory ID = 20131230084 Lab Value = 0.018 Expected Conc. = 0.02 Report level label = 0.014 Pct Recovery = 88% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl SpecificMix = A088380 Laboratory ID = 20130650005 Lab Value = 0.010 Expected Conc. = 0.02 Report level label = 0.014 Pct Recovery = 51% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl SpecificMix = A088380 Laboratory ID = 20130390105 Lab Value = 0.012 Expected Conc. = 0.02 Report level label = 0.014 Pct Recovery = 61% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl SpecificMix = T1120530013 Analysis Date = 02/08/18 Pct Recovery = 77% Analysis Date = 01/29/18 Pct Recovery = 77% Analysis Date = 01/29/18 Pct Recovery = 77% Analysis Date = 01/20/18 Pct Recovery = 76% Analysis Date = 01/20/18 Pct Recovery = 76% Analysis Date = 01/11/18 Pct Recovery = 76% Analysis Date = 01/11/18 Pct Recovery = 76% Analysis Date = 01/02/18 Pct Recovery = 76% Analysis Date = 01/02/18 Pct Recovery = 76% Analysis Date = 12/23/17 Pct Recovery = 76% Analysis Date = 12/23/17 Pct Recovery = 76% Analysis Date = 12/14/17 Pct Recovery = 76% Analysis Date = 12/14/17 Pct Recovery = 76% Analysis Date = 12/05/17 Pct Recovery = 76% Analysis Date = 12/05/17 Pct Recovery = 76% Analysis Date = 11/26/17 Pct Recovery = 75% Analysis Date = 11/26/17 Pct Recovery = 75% Analysis Date = 11/16/17 Pct Recovery = 75% Analysis Date = 11/16/17 Pct Recovery = 75% Analysis Date = 11/07/17 Pct Recovery = 75% Analysis Date = 11/07/17 Pct Recovery = 75% Analysis Date = 10/29/17 Pct Recovery = 75% Analysis Date = 10/29/17 Pct Recovery = 75% Analysis Date = 10/20/17 Pct Recovery = 75% Analysis Date = 10/20/17 Pct Recovery = 75% Analysis Date = 10/10/17 Pct Recovery = 75% Analysis Date = 10/10/17 Pct Recovery = 75% Analysis Date = 10/01/17 Pct Recovery = 75% Analysis Date = 10/01/17 Pct Recovery = 75% Analysis Date = 09/22/17 Pct Recovery = 74% Analysis Date = 09/22/17 Pct Recovery = 74% Analysis Date = 09/13/17 Pct Recovery = 74% Analysis Date = 09/13/17 Pct Recovery = 74% Analysis Date = 09/03/17 Pct Recovery = 74% Analysis Date = 09/03/17 Pct Recovery = 74% Analysis Date = 08/25/17 Pct Recovery = 74% Analysis Date = 08/25/17 Pct Recovery = 74% Analysis Date = 08/16/17 Pct Recovery = 74% Analysis Date = 08/16/17 Pct Recovery = 74% Analysis Date = 08/07/17 Pct Recovery = 74% Analysis Date = 08/07/17 Pct Recovery = 74% Analysis Date = 07/28/17 Pct Recovery = 73% Analysis Date = 07/28/17 Pct Recovery = 73% Analysis Date = 07/19/17 Pct Recovery = 73% Analysis Date = 07/19/17 Pct Recovery = 73% Analysis Date = 07/10/17 Pct Recovery = 73% Analysis Date = 07/10/17 Pct Recovery = 73% Analysis Date = 07/01/17 Pct Recovery = 73% Analysis Date = 07/01/17 Pct Recovery = 73% Analysis Date = 06/21/17 Pct Recovery = 73% Analysis Date = 06/21/17 Pct Recovery = 73% Analysis Date = 06/12/17 Pct Recovery = 73% Analysis Date = 06/12/17 Pct Recovery = 73% Analysis Date = 06/03/17 Pct Recovery = 73% Analysis Date = 06/03/17 Pct Recovery = 73% Analysis Date = 05/25/17 Pct Recovery = 72% Analysis Date = 05/25/17 Pct Recovery = 72% Analysis Date = 05/15/17 Pct Recovery = 72% Analysis Date = 05/15/17 Pct Recovery = 72% Analysis Date = 05/06/17 Pct Recovery = 72% Analysis Date = 05/06/17 Pct Recovery = 72% Analysis Date = 04/27/17 Pct Recovery = 72% Analysis Date = 04/27/17 Pct Recovery = 72% Analysis Date = 04/18/17 Pct Recovery = 72% Analysis Date = 04/18/17 Pct Recovery = 72% Analysis Date = 04/08/17 Pct Recovery = 72% Analysis Date = 04/08/17 Pct Recovery = 72% Analysis Date = 03/30/17 Pct Recovery = 71% Analysis Date = 03/30/17 Pct Recovery = 71% Analysis Date = 03/21/17 Pct Recovery = 71% Analysis Date = 03/21/17 Pct Recovery = 71% Analysis Date = 03/12/17 Pct Recovery = 71% Analysis Date = 03/12/17 Pct Recovery = 71% Analysis Date = 03/02/17 Pct Recovery = 71% Analysis Date = 03/02/17 Pct Recovery = 71% Analysis Date = 02/21/17 Pct Recovery = 71% Analysis Date = 02/21/17 Pct Recovery = 71% Analysis Date = 02/12/17 Pct Recovery = 71% Analysis Date = 02/12/17 Pct Recovery = 71% Analysis Date = 02/03/17 Pct Recovery = 71% Analysis Date = 02/03/17 Pct Recovery = 71% Analysis Date = 01/24/17 Pct Recovery = 70% Analysis Date = 01/24/17 Pct Recovery = 70% Analysis Date = 01/15/17 Pct Recovery = 70% Analysis Date = 01/15/17 Pct Recovery = 70% Analysis Date = 01/06/17 Pct Recovery = 70% Analysis Date = 01/06/17 Pct Recovery = 70% Analysis Date = 12/28/16 Pct Recovery = 70% Analysis Date = 12/28/16 Pct Recovery = 70% Analysis Date = 12/18/16 Pct Recovery = 70% Analysis Date = 12/18/16 Pct Recovery = 70% Analysis Date = 12/09/16 Pct Recovery = 70% Analysis Date = 12/09/16 Pct Recovery = 70% Analysis Date = 11/30/16 Pct Recovery = 70% Analysis Date = 11/30/16 Pct Recovery = 70% Analysis Date = 11/21/16 Pct Recovery = 70% Analysis Date = 11/21/16 Pct Recovery = 70% Analysis Date = 11/11/16 Pct Recovery = 69% Analysis Date = 11/11/16 Pct Recovery = 69% Analysis Date = 11/02/16 Pct Recovery = 69% Analysis Date = 11/02/16 Pct Recovery = 69% Analysis Date = 10/24/16 Pct Recovery = 69% Analysis Date = 10/24/16 Pct Recovery = 69% Analysis Date = 10/15/16 Pct Recovery = 69% Analysis Date = 10/15/16 Pct Recovery = 69% Analysis Date = 10/05/16 Pct Recovery = 69% Analysis Date = 10/05/16 Pct Recovery = 69% Analysis Date = 09/26/16 Pct Recovery = 69% Analysis Date = 09/26/16 Pct Recovery = 69% Analysis Date = 09/17/16 Pct Recovery = 69% Analysis Date = 09/17/16 Pct Recovery = 69% Analysis Date = 09/08/16 Pct Recovery = 69% Analysis Date = 09/08/16 Pct Recovery = 69% Analysis Date = 08/29/16 Pct Recovery = 68% Analysis Date = 08/29/16 Pct Recovery = 68% Analysis Date = 08/20/16 Pct Recovery = 68% Analysis Date = 08/20/16 Pct Recovery = 68% Analysis Date = 08/11/16 Pct Recovery = 68% Analysis Date = 08/11/16 Pct Recovery = 68% Analysis Date = 08/02/16 Pct Recovery = 68% Analysis Date = 08/02/16 Pct Recovery = 68% Analysis Date = 07/23/16 Pct Recovery = 68% Analysis Date = 07/23/16 Pct Recovery = 68% Analysis Date = 07/14/16 Pct Recovery = 68% Analysis Date = 07/14/16 Pct Recovery = 68% Analysis Date = 07/05/16 Pct Recovery = 68% Analysis Date = 07/05/16 Pct Recovery = 68% Analysis Date = 06/26/16 Pct Recovery = 68% Analysis Date = 06/26/16 Pct Recovery = 68% Analysis Date = 06/16/16 Pct Recovery = 67% Analysis Date = 06/16/16 Pct Recovery = 67% Analysis Date = 06/07/16 Pct Recovery = 67% Analysis Date = 06/07/16 Pct Recovery = 67% Analysis Date = 05/29/16 Pct Recovery = 67% Analysis Date = 05/29/16 Pct Recovery = 67% Analysis Date = 05/20/16 Pct Recovery = 67% Analysis Date = 05/20/16 Pct Recovery = 67% Analysis Date = 05/10/16 Pct Recovery = 67% Analysis Date = 05/10/16 Pct Recovery = 67% Analysis Date = 05/01/16 Pct Recovery = 67% Analysis Date = 05/01/16 Pct Recovery = 67% Analysis Date = 04/22/16 Pct Recovery = 67% Analysis Date = 04/22/16 Pct Recovery = 67% Analysis Date = 04/13/16 Pct Recovery = 67% Analysis Date = 04/13/16 Pct Recovery = 67% Analysis Date = 04/03/16 Pct Recovery = 67% Analysis Date = 04/03/16 Pct Recovery = 67% Analysis Date = 03/25/16 Pct Recovery = 67% Analysis Date = 03/25/16 Pct Recovery = 67% Analysis Date = 03/16/16 Pct Recovery = 67% Analysis Date = 03/16/16 Pct Recovery = 67% Analysis Date = 03/07/16 Pct Recovery = 67% Analysis Date = 03/07/16 Pct Recovery = 67% Analysis Date = 02/26/16 Pct Recovery = 67% Analysis Date = 02/26/16 Pct Recovery = 67% Analysis Date = 02/17/16 Pct Recovery = 67% Analysis Date = 02/17/16 Pct Recovery = 67% Analysis Date = 02/08/16 Pct Recovery = 67% Analysis Date = 02/08/16 Pct Recovery = 67% Analysis Date = 01/30/16 Pct Recovery = 67% Analysis Date = 01/30/16 Pct Recovery = 67% Analysis Date = 01/20/16 Pct Recovery = 67% Analysis Date = 01/20/16 Pct Recovery = 67% Analysis Date = 01/11/16 Pct Recovery = 67% Analysis Date = 01/11/16 Pct Recovery = 67% Analysis Date = 01/02/16 Pct Recovery = 67% Analysis Date = 01/02/16 Pct Recovery = 67% Analysis Date = 12/24/15 Pct Recovery = 67% Analysis Date = 12/24/15 Pct Recovery = 67% Analysis Date = 12/14/15 Pct Recovery = 67% Analysis Date = 12/14/15 Pct Recovery = 67% Analysis Date = 12/05/15 Pct Recovery = 67% Analysis Date = 12/05/15 Pct Recovery = 67% Analysis Date = 11/26/15 Pct Recovery = 67% Analysis Date = 11/26/15 Pct Recovery = 67% Analysis Date = 11/17/15 Pct Recovery = 67% Analysis Date = 11/17/15 Pct Recovery = 67% Analysis Date = 11/07/15 Pct Recovery = 67% Analysis Date = 11/07/15 Pct Recovery = 67% Analysis Date = 10/29/15 Pct Recovery = 67% Analysis Date = 10/29/15 Pct Recovery = 67% Analysis Date = 10/20/15 Pct Recovery = 67% Analysis Date = 10/20/15 Pct Recovery = 67% Analysis Date = 10/11/15 Pct Recovery = 67% Analysis Date = 10/11/15 Pct Recovery = 67% Analysis Date = 10/01/15 Pct Recovery = 67% Analysis Date = 10/01/15 Pct Recovery = 67% Analysis Date = 09/22/15 Pct Recovery = 67% Analysis Date = 09/22/15 Pct Recovery = 67% Analysis Date = 09/13/15 Pct Recovery = 67% Analysis Date = 09/13/15 Pct Recovery = 67% Analysis Date = 09/04/15 Pct Recovery = 67% Analysis Date = 09/04/15 Pct Recovery = 67% Analysis Date = 08/25/15 Pct Recovery = 66% Analysis Date = 08/25/15 Pct Recovery = 66% Analysis Date = 08/16/15 Pct Recovery = 66% Analysis Date = 08/16/15 Pct Recovery = 66% Analysis Date = 08/07/15 Pct Recovery = 66% Analysis Date = 08/07/15 Pct Recovery = 66% Analysis Date = 07/29/15 Pct Recovery = 66% Analysis Date = 07/29/15 Pct Recovery = 66% Analysis Date = 07/19/15 Pct Recovery = 66% Analysis Date = 07/19/15 Pct Recovery = 66% Analysis Date = 07/10/15 Pct Recovery = 66% Analysis Date = 07/10/15 Pct Recovery = 66% Analysis Date = 07/01/15 Pct Recovery = 65% Analysis Date = 07/01/15 Pct Recovery = 65% Analysis Date = 06/22/15 Pct Recovery = 65% Analysis Date = 06/22/15 Pct Recovery = 65% Analysis Date = 06/12/15 Pct Recovery = 65% Analysis Date = 06/12/15 Pct Recovery = 65% Analysis Date = 06/03/15 Pct Recovery = 65% Analysis Date = 06/03/15 Pct Recovery = 65% Analysis Date = 05/25/15 Pct Recovery = 65% Analysis Date = 05/25/15 Pct Recovery = 65% Analysis Date = 05/16/15 Pct Recovery = 65% Analysis Date = 05/16/15 Pct Recovery = 65% Analysis Date = 05/06/15 Pct Recovery = 65% Analysis Date = 05/06/15 Pct Recovery = 65% Analysis Date = 04/27/15 Pct Recovery = 65% Analysis Date = 04/27/15 Pct Recovery = 65% Analysis Date = 04/18/15 Pct Recovery = 65% Analysis Date = 04/18/15 Pct Recovery = 65% Analysis Date = 04/09/15 Pct Recovery = 65% Analysis Date = 04/09/15 Pct Recovery = 65% Analysis Date = 03/30/15 Pct Recovery = 65% Analysis Date = 03/30/15 Pct Recovery = 65% Analysis Date = 03/21/15 Pct Recovery = 64% Analysis Date = 03/21/15 Pct Recovery = 64% Analysis Date = 03/12/15 Pct Recovery = 64% Analysis Date = 03/12/15 Pct Recovery = 64% Analysis Date = 03/03/15 Pct Recovery = 64% Analysis Date = 03/03/15 Pct Recovery = 64% Analysis Date = 02/21/15 Pct Recovery = 64% Analysis Date = 02/21/15 Pct Recovery = 64% Analysis Date = 02/12/15 Pct Recovery = 64% Analysis Date = 02/12/15 Pct Recovery = 64% Analysis Date = 02/03/15 Pct Recovery = 64% Analysis Date = 02/03/15 Pct Recovery = 64% Analysis Date = 01/25/15 Pct Recovery = 64% Analysis Date = 01/25/15 Pct Recovery = 64% Analysis Date = 01/15/15 Pct Recovery = 64% Analysis Date = 01/15/15 Pct Recovery = 64% Analysis Date = 01/06/15 Pct Recovery = 64% Analysis Date = 01/06/15 Pct Recovery = 64% Analysis Date = 12/28/14 Pct Recovery = 64% Analysis Date = 12/28/14 Pct Recovery = 64% Analysis Date = 12/19/14 Pct Recovery = 64% Analysis Date = 12/19/14 Pct Recovery = 64% Analysis Date = 12/09/14 Pct Recovery = 64% Analysis Date = 12/09/14 Pct Recovery = 64% Analysis Date = 11/30/14 Pct Recovery = 64% Analysis Date = 11/30/14 Pct Recovery = 64% Analysis Date = 11/21/14 Pct Recovery = 63% Analysis Date = 11/21/14 Pct Recovery = 63% Analysis Date = 11/12/14 Pct Recovery = 63% Analysis Date = 11/12/14 Pct Recovery = 63% Analysis Date = 11/02/14 Pct Recovery = 63% Analysis Date = 11/02/14 Pct Recovery = 63% Analysis Date = 10/24/14 Pct Recovery = 63% Analysis Date = 10/24/14 Pct Recovery = 63% Analysis Date = 10/15/14 Pct Recovery = 63% Analysis Date = 10/15/14 Pct Recovery = 63% Analysis Date = 10/06/14 Pct Recovery = 62% Analysis Date = 10/06/14 Pct Recovery = 62% Analysis Date = 09/26/14 Pct Recovery = 62% Analysis Date = 09/26/14 Pct Recovery = 62% Analysis Date = 09/17/14 Pct Recovery = 62% Analysis Date = 09/17/14 Pct Recovery = 62% Analysis Date = 09/08/14 Pct Recovery = 62% Analysis Date = 09/08/14 Pct Recovery = 62% Analysis Date = 08/30/14 Pct Recovery = 61% Analysis Date = 08/30/14 Pct Recovery = 61% Analysis Date = 08/20/14 Pct Recovery = 61% Analysis Date = 08/20/14 Pct Recovery = 61% Analysis Date = 08/11/14 Pct Recovery = 61% Analysis Date = 08/11/14 Pct Recovery = 61% Analysis Date = 08/02/14 Pct Recovery = 60% Analysis Date = 08/02/14 Pct Recovery = 60% Analysis Date = 07/24/14 Pct Recovery = 60% Analysis Date = 07/24/14 Pct Recovery = 60% Analysis Date = 07/14/14 Pct Recovery = 60% Analysis Date = 07/14/14 Pct Recovery = 60% Analysis Date = 07/05/14 Pct Recovery = 60% Analysis Date = 07/05/14 Pct Recovery = 60% Analysis Date = 06/26/14 Pct Recovery = 59% Analysis Date = 06/26/14 Pct Recovery = 59% Analysis Date = 06/17/14 Pct Recovery = 59% Analysis Date = 06/17/14 Pct Recovery = 59% Analysis Date = 06/07/14 Pct Recovery = 59% Analysis Date = 06/07/14 Pct Recovery = 59% Analysis Date = 05/29/14 Pct Recovery = 59% Analysis Date = 05/29/14 Pct Recovery = 59% Analysis Date = 05/20/14 Pct Recovery = 58% Analysis Date = 05/20/14 Pct Recovery = 58% Analysis Date = 05/11/14 Pct Recovery = 58% Analysis Date = 05/11/14 Pct Recovery = 58% Analysis Date = 05/01/14 Pct Recovery = 58% Analysis Date = 05/01/14 Pct Recovery = 58% Analysis Date = 04/22/14 Pct Recovery = 58% Analysis Date = 04/22/14 Pct Recovery = 58% Analysis Date = 04/13/14 Pct Recovery = 57% Analysis Date = 04/13/14 Pct Recovery = 57% Analysis Date = 04/04/14 Pct Recovery = 57% Analysis Date = 04/04/14 Pct Recovery = 57% Analysis Date = 03/25/14 Pct Recovery = 57% Analysis Date = 03/25/14 Pct Recovery = 57% Analysis Date = 03/16/14 Pct Recovery = 57% Analysis Date = 03/16/14 Pct Recovery = 57% Analysis Date = 03/07/14 Pct Recovery = 57% Analysis Date = 03/07/14 Pct Recovery = 57% Analysis Date = 02/26/14 Pct Recovery = 57% Analysis Date = 02/26/14 Pct Recovery = 57% Analysis Date = 02/16/14 Pct Recovery = 57% Analysis Date = 02/16/14 Pct Recovery = 57% Analysis Date = 02/07/14 Pct Recovery = 57% Analysis Date = 02/07/14 Pct Recovery = 57% Analysis Date = 01/29/14 Pct Recovery = 57% Analysis Date = 01/29/14 Pct Recovery = 57% Analysis Date = 01/20/14 Pct Recovery = 57% Analysis Date = 01/20/14 Pct Recovery = 57% Analysis Date = 01/10/14 Pct Recovery = 57% Analysis Date = 01/10/14 Pct Recovery = 57% Analysis Date = 01/01/14 Pct Recovery = 57% Analysis Date = 01/01/14 Pct Recovery = 57% Analysis Date = 12/23/13 Pct Recovery = 57% Analysis Date = 12/23/13 Pct Recovery = 57% Analysis Date = 12/14/13 Pct Recovery = 57% Analysis Date = 12/14/13 Pct Recovery = 57% Analysis Date = 12/04/13 Pct Recovery = 57% Analysis Date = 12/04/13 Pct Recovery = 57% Analysis Date = 11/25/13 Pct Recovery = 57% Analysis Date = 11/25/13 Pct Recovery = 57% Analysis Date = 11/16/13 Pct Recovery = 57% Analysis Date = 11/16/13 Pct Recovery = 57% Analysis Date = 11/07/13 Pct Recovery = 57% Analysis Date = 11/07/13 Pct Recovery = 57% Analysis Date = 10/28/13 Pct Recovery = 57% Analysis Date = 10/28/13 Pct Recovery = 57% Analysis Date = 10/19/13 Pct Recovery = 57% Analysis Date = 10/19/13 Pct Recovery = 57% Analysis Date = 10/10/13 Pct Recovery = 57% Analysis Date = 10/10/13 Pct Recovery = 57% Analysis Date = 10/01/13 Pct Recovery = 57% Analysis Date = 10/01/13 Pct Recovery = 57% Analysis Date = 09/21/13 Pct Recovery = 57% Analysis Date = 09/21/13 Pct Recovery = 57% Analysis Date = 09/12/13 Pct Recovery = 57% Analysis Date = 09/12/13 Pct Recovery = 57% Analysis Date = 09/03/13 Pct Recovery = 57% Analysis Date = 09/03/13 Pct Recovery = 57% Analysis Date = 08/25/13 Pct Recovery = 57% Analysis Date = 08/25/13 Pct Recovery = 57% Analysis Date = 08/15/13 Pct Recovery = 57% Analysis Date = 08/15/13 Pct Recovery = 57% Analysis Date = 08/06/13 Pct Recovery = 56% Analysis Date = 08/06/13 Pct Recovery = 56% Analysis Date = 07/28/13 Pct Recovery = 56% Analysis Date = 07/28/13 Pct Recovery = 56% Analysis Date = 07/19/13 Pct Recovery = 56% Analysis Date = 07/19/13 Pct Recovery = 56% Analysis Date = 07/09/13 Pct Recovery = 56% Analysis Date = 07/09/13 Pct Recovery = 56% Analysis Date = 06/30/13 Pct Recovery = 56% Analysis Date = 06/30/13 Pct Recovery = 56% Analysis Date = 06/21/13 Pct Recovery = 56% Analysis Date = 06/21/13 Pct Recovery = 56% Analysis Date = 06/12/13 Pct Recovery = 56% Analysis Date = 06/12/13 Pct Recovery = 56% Analysis Date = 06/02/13 Pct Recovery = 56% Analysis Date = 06/02/13 Pct Recovery = 56% Analysis Date = 05/24/13 Pct Recovery = 56% Analysis Date = 05/24/13 Pct Recovery = 56% Analysis Date = 05/15/13 Pct Recovery = 56% Analysis Date = 05/15/13 Pct Recovery = 56% Analysis Date = 05/06/13 Pct Recovery = 56% Analysis Date = 05/06/13 Pct Recovery = 56% Analysis Date = 04/26/13 Pct Recovery = 56% Analysis Date = 04/26/13 Pct Recovery = 56% Analysis Date = 04/17/13 Pct Recovery = 56% Analysis Date = 04/17/13 Pct Recovery = 56% Analysis Date = 04/08/13 Pct Recovery = 56% Analysis Date = 04/08/13 Pct Recovery = 56% Analysis Date = 03/30/13 Pct Recovery = 56% Analysis Date = 03/30/13 Pct Recovery = 56% Analysis Date = 03/20/13 Pct Recovery = 56% Analysis Date = 03/20/13 Pct Recovery = 56% Analysis Date = 03/11/13 Pct Recovery = 56% Analysis Date = 03/11/13 Pct Recovery = 56% Analysis Date = 03/02/13 Pct Recovery = 56% Analysis Date = 03/02/13 Pct Recovery = 56% Analysis Date = 02/21/13 Pct Recovery = 56% Analysis Date = 02/21/13 Pct Recovery = 56% Analysis Date = 02/11/13 Pct Recovery = 56% Analysis Date = 02/11/13 Pct Recovery = 56% Analysis Date = 02/02/13 Pct Recovery = 56% Analysis Date = 02/02/13 Pct Recovery = 56% Analysis Date = 01/24/13 Pct Recovery = 56% Analysis Date = 01/24/13 Pct Recovery = 56% Analysis Date = 01/15/13 Pct Recovery = 56% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
CYHALOTHRIN

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 74 63% 16% 60% 14%
Total 74 63% 16% 60% 14%

Sample Statistics
CYHALOTHRIN

Characteristic N % % Basis
Plotted 74 99% Spiked
Estimated Values 74 99% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 75 .  
False Negatives 1 1% 1 out of 75
Not Spiked 43 .  
False Positives 0 0% 0 out of 43

OBSP Determination:
CYPERMETHRIN
METHOD: 2033 , TESTIDCODE: 61586GCM39

Laboratory ID = 20130250061 Lab Value = 0.171 Expected Conc. = 0.378 Report level label = 0.02 Pct Recovery = 45% Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl SpecificMix = 05BB029 Laboratory ID = 20140100085 Lab Value = 0.192 Expected Conc. = 0.286 Report level label = 0.02 Pct Recovery = 67% Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl SpecificMix = 042413 Laboratory ID = 20140230082 Lab Value = 0.087 Expected Conc. = 0.1885 Report level label = 0.02 Pct Recovery = 46% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl SpecificMix = 012513 Laboratory ID = 20132420001 Lab Value = 0.091 Expected Conc. = 0.1885 Report level label = 0.02 Pct Recovery = 48% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl SpecificMix = 012513 Laboratory ID = 20130940097 Lab Value = 0.093 Expected Conc. = 0.1875 Report level label = 0.02 Pct Recovery = 50% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = 052412 Laboratory ID = 20130100066 Lab Value = 0.113 Expected Conc. = 0.1875 Report level label = 0.02 Pct Recovery = 60% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl SpecificMix = 052412 Laboratory ID = 20132690010 Lab Value = 0.105 Expected Conc. = 0.143 Report level label = 0.02 Pct Recovery = 73% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl SpecificMix = 042413 Laboratory ID = 20132560001 Lab Value = 0.084 Expected Conc. = 0.143 Report level label = 0.02 Pct Recovery = 59% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl SpecificMix = 042413 Laboratory ID = 20132140002 Lab Value = 0.065 Expected Conc. = 0.1425 Report level label = 0.02 Pct Recovery = 46% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl SpecificMix = 04CC101 Laboratory ID = 20162860079 Lab Value = 0.082 Expected Conc. = 0.13 Report level label = 0.02 Pct Recovery = 63% Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl SpecificMix = 5054800 Laboratory ID = 20161880109 Lab Value = 0.121 Expected Conc. = 0.13 Report level label = 0.02 Pct Recovery = 93% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl SpecificMix = 5054800 Laboratory ID = 20163370001 Lab Value = 0.078 Expected Conc. = 0.1253 Report level label = 0.02 Pct Recovery = 62% Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl SpecificMix = LC20138V Laboratory ID = 20152750006 Lab Value = 0.074 Expected Conc. = 0.1208 Report level label = 0.02 Pct Recovery = 61% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl SpecificMix = 040615 Laboratory ID = 20152610011 Lab Value = 0.094 Expected Conc. = 0.1208 Report level label = 0.02 Pct Recovery = 78% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl SpecificMix = 040615 Laboratory ID = 20171380001 Lab Value = 0.059 Expected Conc. = 0.104 Report level label = 0.02 Pct Recovery = 57% Analysis Date = 06/07/17 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 5054800 Laboratory ID = 20170960001 Lab Value = 0.054 Expected Conc. = 0.104 Report level label = 0.02 Pct Recovery = 52% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl SpecificMix = 5054800 Laboratory ID = 20161740258 Lab Value = 0.060 Expected Conc. = 0.104 Report level label = 0.02 Pct Recovery = 58% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 5054800 Laboratory ID = 20171720140 Lab Value = 0.073 Expected Conc. = 0.1002 Report level label = 0.02 Pct Recovery = 73% Analysis Date = 08/31/17 SpikeMix = Supelco LC20138V: 80 µl & Phenova B20160331: 80 µl SpecificMix = LC20138V Laboratory ID = 20170740063 Lab Value = 0.070 Expected Conc. = 0.1002 Report level label = 0.02 Pct Recovery = 70% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl SpecificMix = LC20138V Laboratory ID = 20161470001 Lab Value = 0.093 Expected Conc. = 0.1002 Report level label = 0.02 Pct Recovery = 92% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl SpecificMix = LC20138V Laboratory ID = 20150720069 Lab Value = 0.058 Expected Conc. = 0.0804 Report level label = 0.02 Pct Recovery = 72% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 0227-14-08 Laboratory ID = 20141770149 Lab Value = 0.048 Expected Conc. = 0.0804 Report level label = 0.02 Pct Recovery = 59% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl SpecificMix = 0227-14-08 Laboratory ID = 20141570088 Lab Value = 0.058 Expected Conc. = 0.0804 Report level label = 0.02 Pct Recovery = 72% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl SpecificMix = 0227-14-08 Laboratory ID = 20150430092 Lab Value = 0.057 Expected Conc. = 0.0798 Report level label = 0.02 Pct Recovery = 71% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl SpecificMix = 042814 Laboratory ID = 20143240095 Lab Value = 0.054 Expected Conc. = 0.0798 Report level label = 0.02 Pct Recovery = 68% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl SpecificMix = 042814 Laboratory ID = 20142960086 Lab Value = 0.048 Expected Conc. = 0.0798 Report level label = 0.02 Pct Recovery = 60% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 042814 Laboratory ID = 20142530087 Lab Value = 0.036 Expected Conc. = 0.0798 Report level label = 0.02 Pct Recovery = 44% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl SpecificMix = 042814 Laboratory ID = 20131230084 Lab Value = 0.060 Expected Conc. = 0.0756 Report level label = 0.02 Pct Recovery = 79% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl SpecificMix = 05BB029 Laboratory ID = 20130510051 Lab Value = 0.049 Expected Conc. = 0.0756 Report level label = 0.02 Pct Recovery = 64% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl SpecificMix = 05BB029 Laboratory ID = 20140860102 Lab Value = 0.031 Expected Conc. = 0.0754 Report level label = 0.02 Pct Recovery = 42% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 012513 Laboratory ID = 20131920149 Lab Value = 0.040 Expected Conc. = 0.0754 Report level label = 0.02 Pct Recovery = 53% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl SpecificMix = 012513 Laboratory ID = 20133400002 Lab Value = 0.043 Expected Conc. = 0.075 Report level label = 0.02 Pct Recovery = 57% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = 052412 Laboratory ID = 20132910008 Lab Value = 0.039 Expected Conc. = 0.075 Report level label = 0.02 Pct Recovery = 52% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = 052412 Laboratory ID = 20130650005 Lab Value = 0.042 Expected Conc. = 0.075 Report level label = 0.02 Pct Recovery = 56% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl SpecificMix = 052412 Laboratory ID = 20172230001 Lab Value = 0.055 Expected Conc. = 0.07 Report level label = 0.02 Pct Recovery = 79% Analysis Date = 10/19/17 SpikeMix = ChemService 6472100: 50 µl & Abs 071717Pest: 50 µl SpecificMix = 6472100 Laboratory ID = 20172560101 Lab Value = 0.050 Expected Conc. = 0.0665 Report level label = 0.02 Pct Recovery = 75% Analysis Date = 12/22/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6567600: 50 µl SpecificMix = EN170808006 Laboratory ID = 20172370001 Lab Value = 0.059 Expected Conc. = 0.0665 Report level label = 0.02 Pct Recovery = 88% Analysis Date = 11/18/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6537100: 50 µl SpecificMix = EN170808006 Laboratory ID = 20151900132 Lab Value = 0.051 Expected Conc. = 0.0604 Report level label = 0.02 Pct Recovery = 84% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl SpecificMix = 040615 Laboratory ID = 20151550293 Lab Value = 0.047 Expected Conc. = 0.0604 Report level label = 0.02 Pct Recovery = 78% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl SpecificMix = 040615 Laboratory ID = 20161260151 Lab Value = 0.039 Expected Conc. = 0.06 Report level label = 0.02 Pct Recovery = 65% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = EN150513008 Laboratory ID = 20160770090 Lab Value = 0.045 Expected Conc. = 0.06 Report level label = 0.02 Pct Recovery = 75% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = EN150513008 Laboratory ID = 20153510109 Lab Value = 0.030 Expected Conc. = 0.06 Report level label = 0.02 Pct Recovery = 49% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = EN150513008 Laboratory ID = 20152330039 Lab Value = 0.039 Expected Conc. = 0.06 Report level label = 0.02 Pct Recovery = 65% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl SpecificMix = EN150513008 Laboratory ID = 20133580036 Lab Value = 0.034 Expected Conc. = 0.0572 Report level label = 0.02 Pct Recovery = 59% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 042413 Laboratory ID = 20133190012 Lab Value = 0.066 Expected Conc. = 0.0572 Report level label = 0.02 Pct Recovery = 115% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 042413 Laboratory ID = 20131650073 Lab Value = 0.060 Expected Conc. = 0.0572 Report level label = 0.02 Pct Recovery = 105% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl SpecificMix = 042413 Laboratory ID = 20140730138 Lab Value = 0.025 Expected Conc. = 0.057 Report level label = 0.02 Pct Recovery = 43% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 04CC101 Laboratory ID = 20140510043 Lab Value = 0.033 Expected Conc. = 0.057 Report level label = 0.02 Pct Recovery = 57% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 04CC101 Laboratory ID = 20133310030 Lab Value = 0.058 Expected Conc. = 0.057 Report level label = 0.02 Pct Recovery = 102% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl SpecificMix = 04CC101 Laboratory ID = 20132280016 Lab Value = 0.043 Expected Conc. = 0.057 Report level label = 0.02 Pct Recovery = 75% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl SpecificMix = 04CC101 Laboratory ID = 20131510026 Lab Value = 0.039 Expected Conc. = 0.057 Report level label = 0.02 Pct Recovery = 68% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl SpecificMix = 04CC101 Laboratory ID = 20171940002 Lab Value = 0.036 Expected Conc. = 0.052 Report level label = 0.02 Pct Recovery = 69% Analysis Date = 11/10/17 SpikeMix = ChemService 5054800: 40 µl & NSI 041816: 40 µl SpecificMix = 5054800 Laboratory ID = 20170460061 Lab Value = 0.028 Expected Conc. = 0.052 Report level label = 0.02 Pct Recovery = 53% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl SpecificMix = 5054800 Laboratory ID = 20163560019 Lab Value = 0.043 Expected Conc. = 0.052 Report level label = 0.02 Pct Recovery = 82% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl SpecificMix = 5054800 Laboratory ID = 20162150213 Lab Value = 0.060 Expected Conc. = 0.052 Report level label = 0.02 Pct Recovery = 115% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl SpecificMix = 5054800 Laboratory ID = 20171510080 Lab Value = 0.041 Expected Conc. = 0.0501 Report level label = 0.02 Pct Recovery = 82% Analysis Date = 06/09/17 SpikeMix = Supelco LC20138V: 40 µl & Crescent 03FF076: 40 µl SpecificMix = LC20138V Laboratory ID = 20162520001 Lab Value = 0.054 Expected Conc. = 0.0501 Report level label = 0.02 Pct Recovery = 107% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl SpecificMix = LC20138V Laboratory ID = 20162660005 Lab Value = 0.029 Expected Conc. = 0.0501 Report level label = 0.02 Pct Recovery = 57% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl SpecificMix = LC20138V Laboratory ID = 20162020124 Lab Value = 0.032 Expected Conc. = 0.0501 Report level label = 0.02 Pct Recovery = 63% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl SpecificMix = LC20138V Laboratory ID = 20173120093 Lab Value = 0.032 Expected Conc. = 0.042 Report level label = 0.02 Pct Recovery = 76% Analysis Date = 03/10/18 SpikeMix = ChemService 6472100: 30 µl & ChemService 6537100: 30 µl SpecificMix = 6472100 Laboratory ID = 20141840097 Lab Value = 0.025 Expected Conc. = 0.0402 Report level label = 0.02 Pct Recovery = 63% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20141490205 Lab Value = 0.026 Expected Conc. = 0.0402 Report level label = 0.02 Pct Recovery = 65% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20141420140 Lab Value = 0.029 Expected Conc. = 0.0402 Report level label = 0.02 Pct Recovery = 73% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20141360094 Lab Value = 0.027 Expected Conc. = 0.0402 Report level label = 0.02 Pct Recovery = 67% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20143370094 Lab Value = 0.025 Expected Conc. = 0.0399 Report level label = 0.02 Pct Recovery = 63% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl SpecificMix = 042814 Laboratory ID = 20142820151 Lab Value = 0.038 Expected Conc. = 0.0399 Report level label = 0.02 Pct Recovery = 94% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl SpecificMix = 042814 Laboratory ID = 20142470041 Lab Value = 0.030 Expected Conc. = 0.0399 Report level label = 0.02 Pct Recovery = 75% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl SpecificMix = 042814 Laboratory ID = 20142200164 Lab Value = 0.028 Expected Conc. = 0.0399 Report level label = 0.02 Pct Recovery = 69% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 042814 Laboratory ID = 20161050143 Lab Value = 0.020 Expected Conc. = 0.0302 Report level label = 0.02 Pct Recovery = 67% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Laboratory ID = 20160430111 Lab Value = 0.024 Expected Conc. = 0.0302 Report level label = 0.02 Pct Recovery = 80% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Laboratory ID = 20160070059 Lab Value = 0.019 Expected Conc. = 0.0302 Report level label = 0.02 Pct Recovery = 62% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = 040615 Laboratory ID = 20151380009 Lab Value = 0.024 Expected Conc. = 0.0302 Report level label = 0.02 Pct Recovery = 78% Analysis Date = 05/30/15 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Laboratory ID = 20151210037 Lab Value = 0.031 Expected Conc. = 0.0302 Report level label = 0.02 Pct Recovery = 104% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Laboratory ID = 20160560044 Lab Value = 0.020 Expected Conc. = 0.03 Report level label = 0.02 Pct Recovery = 66% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl SpecificMix = EN150513008 Laboratory ID = 20153160001 Lab Value = 0.019 Expected Conc. = 0.03 Report level label = 0.02 Pct Recovery = 64% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = EN150513008 Laboratory ID = 20153030068 Lab Value = 0.022 Expected Conc. = 0.03 Report level label = 0.02 Pct Recovery = 72% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150513008 Laboratory ID = 20152190003 Lab Value = 0.020 Expected Conc. = 0.03 Report level label = 0.02 Pct Recovery = 65% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150513008 Laboratory ID = 20151480170 Lab Value = 0.030 Expected Conc. = 0.03 Report level label = 0.02 Pct Recovery = 98% Analysis Date = 06/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150513008 Analysis Date = 03/09/18 Pct Recovery = 74% Analysis Date = 02/28/18 Pct Recovery = 74% Analysis Date = 02/28/18 Pct Recovery = 74% Analysis Date = 02/19/18 Pct Recovery = 74% Analysis Date = 02/19/18 Pct Recovery = 74% Analysis Date = 02/09/18 Pct Recovery = 74% Analysis Date = 02/09/18 Pct Recovery = 74% Analysis Date = 01/31/18 Pct Recovery = 74% Analysis Date = 01/31/18 Pct Recovery = 74% Analysis Date = 01/22/18 Pct Recovery = 74% Analysis Date = 01/22/18 Pct Recovery = 74% Analysis Date = 01/12/18 Pct Recovery = 74% Analysis Date = 01/12/18 Pct Recovery = 74% Analysis Date = 01/03/18 Pct Recovery = 74% Analysis Date = 01/03/18 Pct Recovery = 74% Analysis Date = 12/24/17 Pct Recovery = 74% Analysis Date = 12/24/17 Pct Recovery = 74% Analysis Date = 12/15/17 Pct Recovery = 74% Analysis Date = 12/15/17 Pct Recovery = 74% Analysis Date = 12/06/17 Pct Recovery = 74% Analysis Date = 12/06/17 Pct Recovery = 74% Analysis Date = 11/26/17 Pct Recovery = 74% Analysis Date = 11/26/17 Pct Recovery = 74% Analysis Date = 11/17/17 Pct Recovery = 74% Analysis Date = 11/17/17 Pct Recovery = 74% Analysis Date = 11/07/17 Pct Recovery = 74% Analysis Date = 11/07/17 Pct Recovery = 74% Analysis Date = 10/29/17 Pct Recovery = 74% Analysis Date = 10/29/17 Pct Recovery = 74% Analysis Date = 10/20/17 Pct Recovery = 74% Analysis Date = 10/20/17 Pct Recovery = 74% Analysis Date = 10/10/17 Pct Recovery = 74% Analysis Date = 10/10/17 Pct Recovery = 74% Analysis Date = 10/01/17 Pct Recovery = 74% Analysis Date = 10/01/17 Pct Recovery = 74% Analysis Date = 09/21/17 Pct Recovery = 74% Analysis Date = 09/21/17 Pct Recovery = 74% Analysis Date = 09/12/17 Pct Recovery = 74% Analysis Date = 09/12/17 Pct Recovery = 74% Analysis Date = 09/03/17 Pct Recovery = 74% Analysis Date = 09/03/17 Pct Recovery = 74% Analysis Date = 08/24/17 Pct Recovery = 74% Analysis Date = 08/24/17 Pct Recovery = 74% Analysis Date = 08/15/17 Pct Recovery = 74% Analysis Date = 08/15/17 Pct Recovery = 74% Analysis Date = 08/06/17 Pct Recovery = 73% Analysis Date = 08/06/17 Pct Recovery = 73% Analysis Date = 07/27/17 Pct Recovery = 73% Analysis Date = 07/27/17 Pct Recovery = 73% Analysis Date = 07/18/17 Pct Recovery = 73% Analysis Date = 07/18/17 Pct Recovery = 73% Analysis Date = 07/08/17 Pct Recovery = 73% Analysis Date = 07/08/17 Pct Recovery = 73% Analysis Date = 06/29/17 Pct Recovery = 73% Analysis Date = 06/29/17 Pct Recovery = 73% Analysis Date = 06/20/17 Pct Recovery = 73% Analysis Date = 06/20/17 Pct Recovery = 73% Analysis Date = 06/10/17 Pct Recovery = 73% Analysis Date = 06/10/17 Pct Recovery = 73% Analysis Date = 06/01/17 Pct Recovery = 73% Analysis Date = 06/01/17 Pct Recovery = 73% Analysis Date = 05/22/17 Pct Recovery = 73% Analysis Date = 05/22/17 Pct Recovery = 73% Analysis Date = 05/13/17 Pct Recovery = 73% Analysis Date = 05/13/17 Pct Recovery = 73% Analysis Date = 05/04/17 Pct Recovery = 73% Analysis Date = 05/04/17 Pct Recovery = 73% Analysis Date = 04/24/17 Pct Recovery = 73% Analysis Date = 04/24/17 Pct Recovery = 73% Analysis Date = 04/15/17 Pct Recovery = 73% Analysis Date = 04/15/17 Pct Recovery = 73% Analysis Date = 04/05/17 Pct Recovery = 73% Analysis Date = 04/05/17 Pct Recovery = 73% Analysis Date = 03/27/17 Pct Recovery = 73% Analysis Date = 03/27/17 Pct Recovery = 73% Analysis Date = 03/18/17 Pct Recovery = 73% Analysis Date = 03/18/17 Pct Recovery = 73% Analysis Date = 03/08/17 Pct Recovery = 73% Analysis Date = 03/08/17 Pct Recovery = 73% Analysis Date = 02/27/17 Pct Recovery = 73% Analysis Date = 02/27/17 Pct Recovery = 73% Analysis Date = 02/18/17 Pct Recovery = 73% Analysis Date = 02/18/17 Pct Recovery = 73% Analysis Date = 02/08/17 Pct Recovery = 73% Analysis Date = 02/08/17 Pct Recovery = 73% Analysis Date = 01/30/17 Pct Recovery = 73% Analysis Date = 01/30/17 Pct Recovery = 73% Analysis Date = 01/20/17 Pct Recovery = 73% Analysis Date = 01/20/17 Pct Recovery = 73% Analysis Date = 01/11/17 Pct Recovery = 73% Analysis Date = 01/11/17 Pct Recovery = 73% Analysis Date = 01/02/17 Pct Recovery = 73% Analysis Date = 01/02/17 Pct Recovery = 73% Analysis Date = 12/23/16 Pct Recovery = 73% Analysis Date = 12/23/16 Pct Recovery = 73% Analysis Date = 12/14/16 Pct Recovery = 73% Analysis Date = 12/14/16 Pct Recovery = 73% Analysis Date = 12/04/16 Pct Recovery = 73% Analysis Date = 12/04/16 Pct Recovery = 73% Analysis Date = 11/25/16 Pct Recovery = 73% Analysis Date = 11/25/16 Pct Recovery = 73% Analysis Date = 11/16/16 Pct Recovery = 73% Analysis Date = 11/16/16 Pct Recovery = 73% Analysis Date = 11/06/16 Pct Recovery = 73% Analysis Date = 11/06/16 Pct Recovery = 73% Analysis Date = 10/28/16 Pct Recovery = 73% Analysis Date = 10/28/16 Pct Recovery = 73% Analysis Date = 10/18/16 Pct Recovery = 73% Analysis Date = 10/18/16 Pct Recovery = 73% Analysis Date = 10/09/16 Pct Recovery = 73% Analysis Date = 10/09/16 Pct Recovery = 73% Analysis Date = 09/30/16 Pct Recovery = 73% Analysis Date = 09/30/16 Pct Recovery = 73% Analysis Date = 09/20/16 Pct Recovery = 73% Analysis Date = 09/20/16 Pct Recovery = 73% Analysis Date = 09/11/16 Pct Recovery = 73% Analysis Date = 09/11/16 Pct Recovery = 73% Analysis Date = 09/01/16 Pct Recovery = 72% Analysis Date = 09/01/16 Pct Recovery = 72% Analysis Date = 08/23/16 Pct Recovery = 72% Analysis Date = 08/23/16 Pct Recovery = 72% Analysis Date = 08/14/16 Pct Recovery = 73% Analysis Date = 08/14/16 Pct Recovery = 73% Analysis Date = 08/04/16 Pct Recovery = 73% Analysis Date = 08/04/16 Pct Recovery = 73% Analysis Date = 07/26/16 Pct Recovery = 73% Analysis Date = 07/26/16 Pct Recovery = 73% Analysis Date = 07/17/16 Pct Recovery = 73% Analysis Date = 07/17/16 Pct Recovery = 73% Analysis Date = 07/07/16 Pct Recovery = 73% Analysis Date = 07/07/16 Pct Recovery = 73% Analysis Date = 06/28/16 Pct Recovery = 73% Analysis Date = 06/28/16 Pct Recovery = 73% Analysis Date = 06/18/16 Pct Recovery = 73% Analysis Date = 06/18/16 Pct Recovery = 73% Analysis Date = 06/09/16 Pct Recovery = 73% Analysis Date = 06/09/16 Pct Recovery = 73% Analysis Date = 05/31/16 Pct Recovery = 73% Analysis Date = 05/31/16 Pct Recovery = 73% Analysis Date = 05/21/16 Pct Recovery = 73% Analysis Date = 05/21/16 Pct Recovery = 73% Analysis Date = 05/12/16 Pct Recovery = 73% Analysis Date = 05/12/16 Pct Recovery = 73% Analysis Date = 05/02/16 Pct Recovery = 73% Analysis Date = 05/02/16 Pct Recovery = 73% Analysis Date = 04/23/16 Pct Recovery = 73% Analysis Date = 04/23/16 Pct Recovery = 73% Analysis Date = 04/14/16 Pct Recovery = 73% Analysis Date = 04/14/16 Pct Recovery = 73% Analysis Date = 04/04/16 Pct Recovery = 73% Analysis Date = 04/04/16 Pct Recovery = 73% Analysis Date = 03/26/16 Pct Recovery = 73% Analysis Date = 03/26/16 Pct Recovery = 73% Analysis Date = 03/16/16 Pct Recovery = 73% Analysis Date = 03/16/16 Pct Recovery = 73% Analysis Date = 03/07/16 Pct Recovery = 73% Analysis Date = 03/07/16 Pct Recovery = 73% Analysis Date = 02/27/16 Pct Recovery = 73% Analysis Date = 02/27/16 Pct Recovery = 73% Analysis Date = 02/17/16 Pct Recovery = 73% Analysis Date = 02/17/16 Pct Recovery = 73% Analysis Date = 02/08/16 Pct Recovery = 74% Analysis Date = 02/08/16 Pct Recovery = 74% Analysis Date = 01/30/16 Pct Recovery = 74% Analysis Date = 01/30/16 Pct Recovery = 74% Analysis Date = 01/20/16 Pct Recovery = 74% Analysis Date = 01/20/16 Pct Recovery = 74% Analysis Date = 01/11/16 Pct Recovery = 73% Analysis Date = 01/11/16 Pct Recovery = 73% Analysis Date = 01/01/16 Pct Recovery = 73% Analysis Date = 01/01/16 Pct Recovery = 73% Analysis Date = 12/23/15 Pct Recovery = 73% Analysis Date = 12/23/15 Pct Recovery = 73% Analysis Date = 12/14/15 Pct Recovery = 73% Analysis Date = 12/14/15 Pct Recovery = 73% Analysis Date = 12/04/15 Pct Recovery = 73% Analysis Date = 12/04/15 Pct Recovery = 73% Analysis Date = 11/25/15 Pct Recovery = 73% Analysis Date = 11/25/15 Pct Recovery = 73% Analysis Date = 11/15/15 Pct Recovery = 73% Analysis Date = 11/15/15 Pct Recovery = 73% Analysis Date = 11/06/15 Pct Recovery = 73% Analysis Date = 11/06/15 Pct Recovery = 73% Analysis Date = 10/28/15 Pct Recovery = 73% Analysis Date = 10/28/15 Pct Recovery = 73% Analysis Date = 10/18/15 Pct Recovery = 73% Analysis Date = 10/18/15 Pct Recovery = 73% Analysis Date = 10/09/15 Pct Recovery = 73% Analysis Date = 10/09/15 Pct Recovery = 73% Analysis Date = 09/29/15 Pct Recovery = 73% Analysis Date = 09/29/15 Pct Recovery = 73% Analysis Date = 09/20/15 Pct Recovery = 73% Analysis Date = 09/20/15 Pct Recovery = 73% Analysis Date = 09/11/15 Pct Recovery = 72% Analysis Date = 09/11/15 Pct Recovery = 72% Analysis Date = 09/01/15 Pct Recovery = 72% Analysis Date = 09/01/15 Pct Recovery = 72% Analysis Date = 08/23/15 Pct Recovery = 72% Analysis Date = 08/23/15 Pct Recovery = 72% Analysis Date = 08/13/15 Pct Recovery = 72% Analysis Date = 08/13/15 Pct Recovery = 72% Analysis Date = 08/04/15 Pct Recovery = 72% Analysis Date = 08/04/15 Pct Recovery = 72% Analysis Date = 07/26/15 Pct Recovery = 72% Analysis Date = 07/26/15 Pct Recovery = 72% Analysis Date = 07/16/15 Pct Recovery = 72% Analysis Date = 07/16/15 Pct Recovery = 72% Analysis Date = 07/07/15 Pct Recovery = 72% Analysis Date = 07/07/15 Pct Recovery = 72% Analysis Date = 06/28/15 Pct Recovery = 72% Analysis Date = 06/28/15 Pct Recovery = 72% Analysis Date = 06/18/15 Pct Recovery = 72% Analysis Date = 06/18/15 Pct Recovery = 72% Analysis Date = 06/09/15 Pct Recovery = 72% Analysis Date = 06/09/15 Pct Recovery = 72% Analysis Date = 05/30/15 Pct Recovery = 72% Analysis Date = 05/30/15 Pct Recovery = 72% Analysis Date = 05/21/15 Pct Recovery = 72% Analysis Date = 05/21/15 Pct Recovery = 72% Analysis Date = 05/12/15 Pct Recovery = 71% Analysis Date = 05/12/15 Pct Recovery = 71% Analysis Date = 05/02/15 Pct Recovery = 71% Analysis Date = 05/02/15 Pct Recovery = 71% Analysis Date = 04/23/15 Pct Recovery = 71% Analysis Date = 04/23/15 Pct Recovery = 71% Analysis Date = 04/13/15 Pct Recovery = 71% Analysis Date = 04/13/15 Pct Recovery = 71% Analysis Date = 04/04/15 Pct Recovery = 71% Analysis Date = 04/04/15 Pct Recovery = 71% Analysis Date = 03/26/15 Pct Recovery = 71% Analysis Date = 03/26/15 Pct Recovery = 71% Analysis Date = 03/16/15 Pct Recovery = 71% Analysis Date = 03/16/15 Pct Recovery = 71% Analysis Date = 03/07/15 Pct Recovery = 71% Analysis Date = 03/07/15 Pct Recovery = 71% Analysis Date = 02/25/15 Pct Recovery = 71% Analysis Date = 02/25/15 Pct Recovery = 71% Analysis Date = 02/16/15 Pct Recovery = 71% Analysis Date = 02/16/15 Pct Recovery = 71% Analysis Date = 02/07/15 Pct Recovery = 70% Analysis Date = 02/07/15 Pct Recovery = 70% Analysis Date = 01/28/15 Pct Recovery = 70% Analysis Date = 01/28/15 Pct Recovery = 70% Analysis Date = 01/19/15 Pct Recovery = 70% Analysis Date = 01/19/15 Pct Recovery = 70% Analysis Date = 01/10/15 Pct Recovery = 70% Analysis Date = 01/10/15 Pct Recovery = 70% Analysis Date = 12/31/14 Pct Recovery = 70% Analysis Date = 12/31/14 Pct Recovery = 70% Analysis Date = 12/22/14 Pct Recovery = 70% Analysis Date = 12/22/14 Pct Recovery = 70% Analysis Date = 12/12/14 Pct Recovery = 70% Analysis Date = 12/12/14 Pct Recovery = 70% Analysis Date = 12/03/14 Pct Recovery = 70% Analysis Date = 12/03/14 Pct Recovery = 70% Analysis Date = 11/24/14 Pct Recovery = 70% Analysis Date = 11/24/14 Pct Recovery = 70% Analysis Date = 11/14/14 Pct Recovery = 69% Analysis Date = 11/14/14 Pct Recovery = 69% Analysis Date = 11/05/14 Pct Recovery = 69% Analysis Date = 11/05/14 Pct Recovery = 69% Analysis Date = 10/26/14 Pct Recovery = 69% Analysis Date = 10/26/14 Pct Recovery = 69% Analysis Date = 10/17/14 Pct Recovery = 69% Analysis Date = 10/17/14 Pct Recovery = 69% Analysis Date = 10/08/14 Pct Recovery = 69% Analysis Date = 10/08/14 Pct Recovery = 69% Analysis Date = 09/28/14 Pct Recovery = 69% Analysis Date = 09/28/14 Pct Recovery = 69% Analysis Date = 09/19/14 Pct Recovery = 69% Analysis Date = 09/19/14 Pct Recovery = 69% Analysis Date = 09/09/14 Pct Recovery = 69% Analysis Date = 09/09/14 Pct Recovery = 69% Analysis Date = 08/31/14 Pct Recovery = 68% Analysis Date = 08/31/14 Pct Recovery = 68% Analysis Date = 08/22/14 Pct Recovery = 68% Analysis Date = 08/22/14 Pct Recovery = 68% Analysis Date = 08/12/14 Pct Recovery = 68% Analysis Date = 08/12/14 Pct Recovery = 68% Analysis Date = 08/03/14 Pct Recovery = 68% Analysis Date = 08/03/14 Pct Recovery = 68% Analysis Date = 07/25/14 Pct Recovery = 68% Analysis Date = 07/25/14 Pct Recovery = 68% Analysis Date = 07/15/14 Pct Recovery = 68% Analysis Date = 07/15/14 Pct Recovery = 68% Analysis Date = 07/06/14 Pct Recovery = 68% Analysis Date = 07/06/14 Pct Recovery = 68% Analysis Date = 06/26/14 Pct Recovery = 67% Analysis Date = 06/26/14 Pct Recovery = 67% Analysis Date = 06/17/14 Pct Recovery = 67% Analysis Date = 06/17/14 Pct Recovery = 67% Analysis Date = 06/08/14 Pct Recovery = 67% Analysis Date = 06/08/14 Pct Recovery = 67% Analysis Date = 05/29/14 Pct Recovery = 66% Analysis Date = 05/29/14 Pct Recovery = 66% Analysis Date = 05/20/14 Pct Recovery = 66% Analysis Date = 05/20/14 Pct Recovery = 66% Analysis Date = 05/10/14 Pct Recovery = 66% Analysis Date = 05/10/14 Pct Recovery = 66% Analysis Date = 05/01/14 Pct Recovery = 66% Analysis Date = 05/01/14 Pct Recovery = 66% Analysis Date = 04/22/14 Pct Recovery = 66% Analysis Date = 04/22/14 Pct Recovery = 66% Analysis Date = 04/12/14 Pct Recovery = 66% Analysis Date = 04/12/14 Pct Recovery = 66% Analysis Date = 04/03/14 Pct Recovery = 66% Analysis Date = 04/03/14 Pct Recovery = 66% Analysis Date = 03/24/14 Pct Recovery = 66% Analysis Date = 03/24/14 Pct Recovery = 66% Analysis Date = 03/15/14 Pct Recovery = 66% Analysis Date = 03/15/14 Pct Recovery = 66% Analysis Date = 03/06/14 Pct Recovery = 66% Analysis Date = 03/06/14 Pct Recovery = 66% Analysis Date = 02/24/14 Pct Recovery = 66% Analysis Date = 02/24/14 Pct Recovery = 66% Analysis Date = 02/15/14 Pct Recovery = 65% Analysis Date = 02/15/14 Pct Recovery = 65% Analysis Date = 02/05/14 Pct Recovery = 65% Analysis Date = 02/05/14 Pct Recovery = 65% Analysis Date = 01/27/14 Pct Recovery = 65% Analysis Date = 01/27/14 Pct Recovery = 65% Analysis Date = 01/18/14 Pct Recovery = 65% Analysis Date = 01/18/14 Pct Recovery = 65% Analysis Date = 01/08/14 Pct Recovery = 65% Analysis Date = 01/08/14 Pct Recovery = 65% Analysis Date = 12/30/13 Pct Recovery = 65% Analysis Date = 12/30/13 Pct Recovery = 65% Analysis Date = 12/21/13 Pct Recovery = 65% Analysis Date = 12/21/13 Pct Recovery = 65% Analysis Date = 12/11/13 Pct Recovery = 65% Analysis Date = 12/11/13 Pct Recovery = 65% Analysis Date = 12/02/13 Pct Recovery = 65% Analysis Date = 12/02/13 Pct Recovery = 65% Analysis Date = 11/22/13 Pct Recovery = 65% Analysis Date = 11/22/13 Pct Recovery = 65% Analysis Date = 11/13/13 Pct Recovery = 65% Analysis Date = 11/13/13 Pct Recovery = 65% Analysis Date = 11/04/13 Pct Recovery = 65% Analysis Date = 11/04/13 Pct Recovery = 65% Analysis Date = 10/25/13 Pct Recovery = 64% Analysis Date = 10/25/13 Pct Recovery = 64% Analysis Date = 10/16/13 Pct Recovery = 64% Analysis Date = 10/16/13 Pct Recovery = 64% Analysis Date = 10/06/13 Pct Recovery = 64% Analysis Date = 10/06/13 Pct Recovery = 64% Analysis Date = 09/27/13 Pct Recovery = 64% Analysis Date = 09/27/13 Pct Recovery = 64% Analysis Date = 09/18/13 Pct Recovery = 64% Analysis Date = 09/18/13 Pct Recovery = 64% Analysis Date = 09/08/13 Pct Recovery = 64% Analysis Date = 09/08/13 Pct Recovery = 64% Analysis Date = 08/30/13 Pct Recovery = 64% Analysis Date = 08/30/13 Pct Recovery = 64% Analysis Date = 08/20/13 Pct Recovery = 64% Analysis Date = 08/20/13 Pct Recovery = 64% Analysis Date = 08/11/13 Pct Recovery = 64% Analysis Date = 08/11/13 Pct Recovery = 64% Analysis Date = 08/02/13 Pct Recovery = 64% Analysis Date = 08/02/13 Pct Recovery = 64% Analysis Date = 07/23/13 Pct Recovery = 64% Analysis Date = 07/23/13 Pct Recovery = 64% Analysis Date = 07/14/13 Pct Recovery = 64% Analysis Date = 07/14/13 Pct Recovery = 64% Analysis Date = 07/05/13 Pct Recovery = 64% Analysis Date = 07/05/13 Pct Recovery = 64% Analysis Date = 06/25/13 Pct Recovery = 64% Analysis Date = 06/25/13 Pct Recovery = 64% Analysis Date = 06/16/13 Pct Recovery = 64% Analysis Date = 06/16/13 Pct Recovery = 64% Analysis Date = 06/06/13 Pct Recovery = 64% Analysis Date = 06/06/13 Pct Recovery = 64% Analysis Date = 05/28/13 Pct Recovery = 63% Analysis Date = 05/28/13 Pct Recovery = 63% Analysis Date = 05/19/13 Pct Recovery = 63% Analysis Date = 05/19/13 Pct Recovery = 63% Analysis Date = 05/09/13 Pct Recovery = 63% Analysis Date = 05/09/13 Pct Recovery = 63% Analysis Date = 04/30/13 Pct Recovery = 63% Analysis Date = 04/30/13 Pct Recovery = 63% Analysis Date = 04/20/13 Pct Recovery = 63% Analysis Date = 04/20/13 Pct Recovery = 63% Analysis Date = 04/11/13 Pct Recovery = 63% Analysis Date = 04/11/13 Pct Recovery = 63% Analysis Date = 04/02/13 Pct Recovery = 63% Analysis Date = 04/02/13 Pct Recovery = 63% Analysis Date = 03/23/13 Pct Recovery = 63% Analysis Date = 03/23/13 Pct Recovery = 63% Analysis Date = 03/14/13 Pct Recovery = 63% Analysis Date = 03/14/13 Pct Recovery = 63% Analysis Date = 03/04/13 Pct Recovery = 63% Analysis Date = 03/04/13 Pct Recovery = 63% Analysis Date = 02/23/13 Pct Recovery = 63% Analysis Date = 02/23/13 Pct Recovery = 63% Analysis Date = 02/14/13 Pct Recovery = 63% Analysis Date = 02/14/13 Pct Recovery = 63% Analysis Date = 02/04/13 Pct Recovery = 63% Analysis Date = 02/04/13 Pct Recovery = 63% Analysis Date = 01/26/13 Pct Recovery = 63% Analysis Date = 01/26/13 Pct Recovery = 63% Analysis Date = 01/17/13 Pct Recovery = 63% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
CYPERMETHRIN

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 78 69% 17% 67% 14%
Total 78 69% 17% 67% 14%

Sample Statistics
CYPERMETHRIN

Characteristic N % % Basis
Plotted 78 100% Spiked
Estimated Values 78 100% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 78 .  
False Negatives 0 0% 0 out of 78
Not Spiked 40 .  
False Positives 0 0% 0 out of 40

OBSP Determination:
DACTHAL
METHOD: 2033 , TESTIDCODE: 82682GCM35

Laboratory ID = 20130250061 Lab Value = 0.147 Expected Conc. = 0.15 Report level label = 0.0076 Pct Recovery = 98% Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl SpecificMix = A088380 Laboratory ID = 20140230082 Lab Value = 0.071 Expected Conc. = 0.075 Report level label = 0.0076 Pct Recovery = 95% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl SpecificMix = A093651 Laboratory ID = 20132420001 Lab Value = 0.074 Expected Conc. = 0.075 Report level label = 0.0076 Pct Recovery = 99% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl SpecificMix = A093651 Laboratory ID = 20130810108 Lab Value = 0.071 Expected Conc. = 0.075 Report level label = 0.0076 Pct Recovery = 95% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl SpecificMix = T1120530013 Laboratory ID = 20123560092 Lab Value = 0.075 Expected Conc. = 0.075 Report level label = 0.0076 Pct Recovery = 100% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = T1120530013 Laboratory ID = 20140100085 Lab Value = 0.077 Expected Conc. = 0.07 Report level label = 0.0076 Pct Recovery = 111% Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl SpecificMix = T1130514013 Laboratory ID = 20132490342 Lab Value = 0.088 Expected Conc. = 0.07 Report level label = 0.0076 Pct Recovery = 126% Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl SpecificMix = T1130514013 Laboratory ID = 20180390003 Lab Value = 0.055 Expected Conc. = 0.051 Report level label = 0.0076 Pct Recovery = 108% Analysis Date = 04/06/18 SpikeMix = Spex Organics EN170808006: 100 µl & Abs 071717Pest: 100 µl SpecificMix = 071717Pest Laboratory ID = 20172510330 Lab Value = 0.048 Expected Conc. = 0.051 Report level label = 0.0076 Pct Recovery = 94% Analysis Date = 12/29/17 SpikeMix = ChemService 6537100: 100 µl & Abs 071817Pest: 100 µl SpecificMix = 6537100 Laboratory ID = 20162860079 Lab Value = 0.055 Expected Conc. = 0.048 Report level label = 0.0076 Pct Recovery = 114% Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl SpecificMix = 060916 Laboratory ID = 20163150006 Lab Value = 0.049 Expected Conc. = 0.048 Report level label = 0.0076 Pct Recovery = 102% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl SpecificMix = 060916 Laboratory ID = 20152750006 Lab Value = 0.045 Expected Conc. = 0.0456 Report level label = 0.0076 Pct Recovery = 99% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl SpecificMix = 040615 Laboratory ID = 20152610011 Lab Value = 0.057 Expected Conc. = 0.0456 Report level label = 0.0076 Pct Recovery = 125% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl SpecificMix = 040615 Laboratory ID = 20171660002 Lab Value = 0.041 Expected Conc. = 0.0384 Report level label = 0.0076 Pct Recovery = 107% Analysis Date = 08/23/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = 060916 Laboratory ID = 20171380001 Lab Value = 0.029 Expected Conc. = 0.0384 Report level label = 0.0076 Pct Recovery = 77% Analysis Date = 06/07/17 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 041816 Laboratory ID = 20170740063 Lab Value = 0.036 Expected Conc. = 0.0384 Report level label = 0.0076 Pct Recovery = 92% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl SpecificMix = 041816 Laboratory ID = 20170190026 Lab Value = 0.040 Expected Conc. = 0.0384 Report level label = 0.0076 Pct Recovery = 104% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = 060916 Laboratory ID = 20161740258 Lab Value = 0.030 Expected Conc. = 0.0384 Report level label = 0.0076 Pct Recovery = 78% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 041816 Laboratory ID = 20131370001 Lab Value = 0.047 Expected Conc. = 0.038 Report level label = 0.0076 Pct Recovery = 122% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl SpecificMix = 1473000 Laboratory ID = 20140370077 Lab Value = 0.037 Expected Conc. = 0.035 Report level label = 0.0076 Pct Recovery = 105% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl SpecificMix = T1130514013 Laboratory ID = 20132690010 Lab Value = 0.047 Expected Conc. = 0.035 Report level label = 0.0076 Pct Recovery = 135% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl SpecificMix = T1130514013 Laboratory ID = 20142720002 Lab Value = 0.030 Expected Conc. = 0.0306 Report level label = 0.0076 Pct Recovery = 97% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl SpecificMix = LC06435 Laboratory ID = 20142530087 Lab Value = 0.030 Expected Conc. = 0.0306 Report level label = 0.0076 Pct Recovery = 97% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl SpecificMix = LC06435 Laboratory ID = 20141570088 Lab Value = 0.033 Expected Conc. = 0.0306 Report level label = 0.0076 Pct Recovery = 107% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl SpecificMix = LC06435 Laboratory ID = 20141220025 Lab Value = 0.034 Expected Conc. = 0.0306 Report level label = 0.0076 Pct Recovery = 112% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl SpecificMix = LC06435 Laboratory ID = 20150720069 Lab Value = 0.033 Expected Conc. = 0.03 Report level label = 0.0076 Pct Recovery = 110% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 03DD006 Laboratory ID = 20143110108 Lab Value = 0.027 Expected Conc. = 0.03 Report level label = 0.0076 Pct Recovery = 89% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 03DD006 Laboratory ID = 20142960086 Lab Value = 0.030 Expected Conc. = 0.03 Report level label = 0.0076 Pct Recovery = 99% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 03DD006 Laboratory ID = 20142270001 Lab Value = 0.029 Expected Conc. = 0.03 Report level label = 0.0076 Pct Recovery = 98% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl SpecificMix = 03DD006 Laboratory ID = 20140860102 Lab Value = 0.026 Expected Conc. = 0.03 Report level label = 0.0076 Pct Recovery = 87% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl SpecificMix = A093651 Laboratory ID = 20133400002 Lab Value = 0.033 Expected Conc. = 0.03 Report level label = 0.0076 Pct Recovery = 109% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = A093651 Laboratory ID = 20132910008 Lab Value = 0.028 Expected Conc. = 0.03 Report level label = 0.0076 Pct Recovery = 92% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = A093651 Laboratory ID = 20131920149 Lab Value = 0.029 Expected Conc. = 0.03 Report level label = 0.0076 Pct Recovery = 97% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl SpecificMix = A093651 Laboratory ID = 20131230084 Lab Value = 0.035 Expected Conc. = 0.03 Report level label = 0.0076 Pct Recovery = 117% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl SpecificMix = A088380 Laboratory ID = 20130650005 Lab Value = 0.023 Expected Conc. = 0.03 Report level label = 0.0076 Pct Recovery = 76% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl SpecificMix = A088380 Laboratory ID = 20130390105 Lab Value = 0.023 Expected Conc. = 0.03 Report level label = 0.0076 Pct Recovery = 75% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl SpecificMix = T1120530013 Laboratory ID = 20173480003 Lab Value = 0.025 Expected Conc. = 0.0255 Report level label = 0.0076 Pct Recovery = 97% Analysis Date = 04/05/18 SpikeMix = Abs 071717Pest: 50 µl & ChemService 6567600: 50 µl SpecificMix = 071717Pest Laboratory ID = 20172370001 Lab Value = 0.024 Expected Conc. = 0.0255 Report level label = 0.0076 Pct Recovery = 96% Analysis Date = 11/18/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6537100: 50 µl SpecificMix = 6537100 Laboratory ID = 20172230001 Lab Value = 0.030 Expected Conc. = 0.0255 Report level label = 0.0076 Pct Recovery = 116% Analysis Date = 10/19/17 SpikeMix = ChemService 6472100: 50 µl & Abs 071717Pest: 50 µl SpecificMix = 071717Pest Laboratory ID = 20161260151 Lab Value = 0.021 Expected Conc. = 0.0228 Report level label = 0.0076 Pct Recovery = 93% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = EN150513008 Laboratory ID = 20160770090 Lab Value = 0.020 Expected Conc. = 0.0228 Report level label = 0.0076 Pct Recovery = 89% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = EN150513008 Laboratory ID = 20153510109 Lab Value = 0.019 Expected Conc. = 0.0228 Report level label = 0.0076 Pct Recovery = 85% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = EN150513008 Laboratory ID = 20152330039 Lab Value = 0.024 Expected Conc. = 0.0228 Report level label = 0.0076 Pct Recovery = 106% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl SpecificMix = EN150513008 Laboratory ID = 20151900132 Lab Value = 0.023 Expected Conc. = 0.0228 Report level label = 0.0076 Pct Recovery = 102% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl SpecificMix = 040615 Laboratory ID = 20151550293 Lab Value = 0.027 Expected Conc. = 0.0228 Report level label = 0.0076 Pct Recovery = 117% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl SpecificMix = 040615 Laboratory ID = 20172020035 Lab Value = 0.024 Expected Conc. = 0.0204 Report level label = 0.0076 Pct Recovery = 117% Analysis Date = 11/07/17 SpikeMix = Abs 071717Pest: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 071717Pest Laboratory ID = 20171940002 Lab Value = 0.017 Expected Conc. = 0.0192 Report level label = 0.0076 Pct Recovery = 86% Analysis Date = 11/10/17 SpikeMix = ChemService 5054800: 40 µl & NSI 041816: 40 µl SpecificMix = 041816 Laboratory ID = 20171160110 Lab Value = 0.019 Expected Conc. = 0.0192 Report level label = 0.0076 Pct Recovery = 100% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = 060916 Laboratory ID = 20162520001 Lab Value = 0.020 Expected Conc. = 0.0192 Report level label = 0.0076 Pct Recovery = 102% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl SpecificMix = 060916 Laboratory ID = 20163560019 Lab Value = 0.017 Expected Conc. = 0.0192 Report level label = 0.0076 Pct Recovery = 91% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl SpecificMix = 060916 Laboratory ID = 20162380004 Lab Value = 0.019 Expected Conc. = 0.0192 Report level label = 0.0076 Pct Recovery = 101% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = 060916 Laboratory ID = 20162020124 Lab Value = 0.016 Expected Conc. = 0.0192 Report level label = 0.0076 Pct Recovery = 84% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl SpecificMix = 041816 Laboratory ID = 20161600087 Lab Value = 0.018 Expected Conc. = 0.0192 Report level label = 0.0076 Pct Recovery = 93% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 041816 Laboratory ID = 20161340228 Lab Value = 0.016 Expected Conc. = 0.0192 Report level label = 0.0076 Pct Recovery = 84% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl SpecificMix = 041816 Laboratory ID = 20161190075 Lab Value = 0.015 Expected Conc. = 0.0192 Report level label = 0.0076 Pct Recovery = 80% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 041816 Laboratory ID = 20180940080 Lab Value = 0.014 Expected Conc. = 0.0153 Report level label = 0.0076 Pct Recovery = 94% Analysis Date = 05/31/18 SpikeMix = ChemService 6472100: 30 µl & Abs 071717Pest: 30 µl SpecificMix = 071717Pest Laboratory ID = 20180730064 Lab Value = 0.018 Expected Conc. = 0.0153 Report level label = 0.0076 Pct Recovery = 120% Analysis Date = 05/16/18 SpikeMix = Abs 071717Pest: 30 µl & Abs 071817Pest: 30 µl SpecificMix = 071717Pest Laboratory ID = 20173120093 Lab Value = 0.016 Expected Conc. = 0.0153 Report level label = 0.0076 Pct Recovery = 103% Analysis Date = 03/10/18 SpikeMix = ChemService 6472100: 30 µl & ChemService 6537100: 30 µl SpecificMix = 6537100 Laboratory ID = 20172780018 Lab Value = 0.013 Expected Conc. = 0.0153 Report level label = 0.0076 Pct Recovery = 86% Analysis Date = 02/08/18 SpikeMix = ChemService 6537100: 30 µl & Abs 071817Pest: 30 µl SpecificMix = 6537100 Laboratory ID = 20150150115 Lab Value = 0.014 Expected Conc. = 0.0153 Report level label = 0.0076 Pct Recovery = 93% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl SpecificMix = LC06435 Laboratory ID = 20143370094 Lab Value = 0.012 Expected Conc. = 0.0153 Report level label = 0.0076 Pct Recovery = 75% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl SpecificMix = LC06435 Laboratory ID = 20141910243 Lab Value = 0.014 Expected Conc. = 0.0153 Report level label = 0.0076 Pct Recovery = 93% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = LC06435 Laboratory ID = 20141840097 Lab Value = 0.016 Expected Conc. = 0.0153 Report level label = 0.0076 Pct Recovery = 103% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl SpecificMix = LC06435 Laboratory ID = 20140730138 Lab Value = 0.016 Expected Conc. = 0.0152 Report level label = 0.0076 Pct Recovery = 103% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 1473000 Laboratory ID = 20133470008 Lab Value = 0.017 Expected Conc. = 0.0152 Report level label = 0.0076 Pct Recovery = 113% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl SpecificMix = 1473000 Laboratory ID = 20133310030 Lab Value = 0.016 Expected Conc. = 0.0152 Report level label = 0.0076 Pct Recovery = 103% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl SpecificMix = 1473000 Laboratory ID = 20131790009 Lab Value = 0.019 Expected Conc. = 0.0152 Report level label = 0.0076 Pct Recovery = 122% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl SpecificMix = 1473000 Laboratory ID = 20131650073 Lab Value = 0.018 Expected Conc. = 0.0152 Report level label = 0.0076 Pct Recovery = 118% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl SpecificMix = 1473000 Laboratory ID = 20142200164 Lab Value = 0.015 Expected Conc. = 0.015 Report level label = 0.0076 Pct Recovery = 100% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 03DD006 Laboratory ID = 20141640076 Lab Value = 0.015 Expected Conc. = 0.015 Report level label = 0.0076 Pct Recovery = 102% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = 03DD006 Laboratory ID = 20141420140 Lab Value = 0.016 Expected Conc. = 0.015 Report level label = 0.0076 Pct Recovery = 103% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 03DD006 Laboratory ID = 20141080004 Lab Value = 0.014 Expected Conc. = 0.015 Report level label = 0.0076 Pct Recovery = 95% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl SpecificMix = 03DD006 Laboratory ID = 20133050050 Lab Value = 0.017 Expected Conc. = 0.014 Report level label = 0.0076 Pct Recovery = 120% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl SpecificMix = T1130514013 Laboratory ID = 20132280016 Lab Value = 0.015 Expected Conc. = 0.014 Report level label = 0.0076 Pct Recovery = 108% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl SpecificMix = T1130514013 Laboratory ID = 20161050143 Lab Value = 0.011 Expected Conc. = 0.0114 Report level label = 0.0076 Pct Recovery = 97% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Laboratory ID = 20160430111 Lab Value = 0.012 Expected Conc. = 0.0114 Report level label = 0.0076 Pct Recovery = 106% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Laboratory ID = 20160560044 Lab Value = 0.010 Expected Conc. = 0.0114 Report level label = 0.0076 Pct Recovery = 91% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl SpecificMix = EN150513008 Laboratory ID = 20160070059 Lab Value = 0.011 Expected Conc. = 0.0114 Report level label = 0.0076 Pct Recovery = 95% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = 040615 Laboratory ID = 20153160001 Lab Value = 0.011 Expected Conc. = 0.0114 Report level label = 0.0076 Pct Recovery = 98% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = EN150513008 Laboratory ID = 20153030068 Lab Value = 0.011 Expected Conc. = 0.0114 Report level label = 0.0076 Pct Recovery = 98% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150513008 Laboratory ID = 20152190003 Lab Value = 0.011 Expected Conc. = 0.0114 Report level label = 0.0076 Pct Recovery = 97% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150513008 Laboratory ID = 20151480170 Lab Value = 0.010 Expected Conc. = 0.0114 Report level label = 0.0076 Pct Recovery = 90% Analysis Date = 06/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150513008 Laboratory ID = 20151380009 Lab Value = 0.010 Expected Conc. = 0.0114 Report level label = 0.0076 Pct Recovery = 90% Analysis Date = 05/30/15 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Laboratory ID = 20151210037 Lab Value = 0.011 Expected Conc. = 0.0114 Report level label = 0.0076 Pct Recovery = 97% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Analysis Date = 05/31/18 Pct Recovery = 102% Analysis Date = 05/21/18 Pct Recovery = 102% Analysis Date = 05/21/18 Pct Recovery = 102% Analysis Date = 05/11/18 Pct Recovery = 101% Analysis Date = 05/11/18 Pct Recovery = 101% Analysis Date = 05/01/18 Pct Recovery = 101% Analysis Date = 05/01/18 Pct Recovery = 101% Analysis Date = 04/21/18 Pct Recovery = 101% Analysis Date = 04/21/18 Pct Recovery = 101% Analysis Date = 04/11/18 Pct Recovery = 101% Analysis Date = 04/11/18 Pct Recovery = 101% Analysis Date = 04/02/18 Pct Recovery = 101% Analysis Date = 04/02/18 Pct Recovery = 101% Analysis Date = 03/23/18 Pct Recovery = 101% Analysis Date = 03/23/18 Pct Recovery = 101% Analysis Date = 03/13/18 Pct Recovery = 101% Analysis Date = 03/13/18 Pct Recovery = 101% Analysis Date = 03/03/18 Pct Recovery = 101% Analysis Date = 03/03/18 Pct Recovery = 101% Analysis Date = 02/21/18 Pct Recovery = 101% Analysis Date = 02/21/18 Pct Recovery = 101% Analysis Date = 02/12/18 Pct Recovery = 101% Analysis Date = 02/12/18 Pct Recovery = 101% Analysis Date = 02/02/18 Pct Recovery = 101% Analysis Date = 02/02/18 Pct Recovery = 101% Analysis Date = 01/23/18 Pct Recovery = 100% Analysis Date = 01/23/18 Pct Recovery = 100% Analysis Date = 01/13/18 Pct Recovery = 100% Analysis Date = 01/13/18 Pct Recovery = 100% Analysis Date = 01/03/18 Pct Recovery = 100% Analysis Date = 01/03/18 Pct Recovery = 100% Analysis Date = 12/25/17 Pct Recovery = 100% Analysis Date = 12/25/17 Pct Recovery = 100% Analysis Date = 12/15/17 Pct Recovery = 100% Analysis Date = 12/15/17 Pct Recovery = 100% Analysis Date = 12/05/17 Pct Recovery = 100% Analysis Date = 12/05/17 Pct Recovery = 100% Analysis Date = 11/25/17 Pct Recovery = 100% Analysis Date = 11/25/17 Pct Recovery = 100% Analysis Date = 11/15/17 Pct Recovery = 100% Analysis Date = 11/15/17 Pct Recovery = 100% Analysis Date = 11/05/17 Pct Recovery = 100% Analysis Date = 11/05/17 Pct Recovery = 100% Analysis Date = 10/27/17 Pct Recovery = 100% Analysis Date = 10/27/17 Pct Recovery = 100% Analysis Date = 10/17/17 Pct Recovery = 99% Analysis Date = 10/17/17 Pct Recovery = 99% Analysis Date = 10/07/17 Pct Recovery = 99% Analysis Date = 10/07/17 Pct Recovery = 99% Analysis Date = 09/27/17 Pct Recovery = 99% Analysis Date = 09/27/17 Pct Recovery = 99% Analysis Date = 09/17/17 Pct Recovery = 99% Analysis Date = 09/17/17 Pct Recovery = 99% Analysis Date = 09/08/17 Pct Recovery = 99% Analysis Date = 09/08/17 Pct Recovery = 99% Analysis Date = 08/29/17 Pct Recovery = 99% Analysis Date = 08/29/17 Pct Recovery = 99% Analysis Date = 08/19/17 Pct Recovery = 99% Analysis Date = 08/19/17 Pct Recovery = 99% Analysis Date = 08/09/17 Pct Recovery = 99% Analysis Date = 08/09/17 Pct Recovery = 99% Analysis Date = 07/30/17 Pct Recovery = 99% Analysis Date = 07/30/17 Pct Recovery = 99% Analysis Date = 07/21/17 Pct Recovery = 99% Analysis Date = 07/21/17 Pct Recovery = 99% Analysis Date = 07/11/17 Pct Recovery = 99% Analysis Date = 07/11/17 Pct Recovery = 99% Analysis Date = 07/01/17 Pct Recovery = 99% Analysis Date = 07/01/17 Pct Recovery = 99% Analysis Date = 06/21/17 Pct Recovery = 98% Analysis Date = 06/21/17 Pct Recovery = 98% Analysis Date = 06/11/17 Pct Recovery = 98% Analysis Date = 06/11/17 Pct Recovery = 98% Analysis Date = 06/02/17 Pct Recovery = 98% Analysis Date = 06/02/17 Pct Recovery = 98% Analysis Date = 05/23/17 Pct Recovery = 98% Analysis Date = 05/23/17 Pct Recovery = 98% Analysis Date = 05/13/17 Pct Recovery = 98% Analysis Date = 05/13/17 Pct Recovery = 98% Analysis Date = 05/03/17 Pct Recovery = 98% Analysis Date = 05/03/17 Pct Recovery = 98% Analysis Date = 04/23/17 Pct Recovery = 98% Analysis Date = 04/23/17 Pct Recovery = 98% Analysis Date = 04/13/17 Pct Recovery = 98% Analysis Date = 04/13/17 Pct Recovery = 98% Analysis Date = 04/04/17 Pct Recovery = 98% Analysis Date = 04/04/17 Pct Recovery = 98% Analysis Date = 03/25/17 Pct Recovery = 98% Analysis Date = 03/25/17 Pct Recovery = 98% Analysis Date = 03/15/17 Pct Recovery = 98% Analysis Date = 03/15/17 Pct Recovery = 98% Analysis Date = 03/05/17 Pct Recovery = 98% Analysis Date = 03/05/17 Pct Recovery = 98% Analysis Date = 02/23/17 Pct Recovery = 98% Analysis Date = 02/23/17 Pct Recovery = 98% Analysis Date = 02/14/17 Pct Recovery = 97% Analysis Date = 02/14/17 Pct Recovery = 97% Analysis Date = 02/04/17 Pct Recovery = 97% Analysis Date = 02/04/17 Pct Recovery = 97% Analysis Date = 01/25/17 Pct Recovery = 97% Analysis Date = 01/25/17 Pct Recovery = 97% Analysis Date = 01/15/17 Pct Recovery = 97% Analysis Date = 01/15/17 Pct Recovery = 97% Analysis Date = 01/05/17 Pct Recovery = 97% Analysis Date = 01/05/17 Pct Recovery = 97% Analysis Date = 12/27/16 Pct Recovery = 97% Analysis Date = 12/27/16 Pct Recovery = 97% Analysis Date = 12/17/16 Pct Recovery = 97% Analysis Date = 12/17/16 Pct Recovery = 97% Analysis Date = 12/07/16 Pct Recovery = 97% Analysis Date = 12/07/16 Pct Recovery = 97% Analysis Date = 11/27/16 Pct Recovery = 97% Analysis Date = 11/27/16 Pct Recovery = 97% Analysis Date = 11/17/16 Pct Recovery = 97% Analysis Date = 11/17/16 Pct Recovery = 97% Analysis Date = 11/08/16 Pct Recovery = 97% Analysis Date = 11/08/16 Pct Recovery = 97% Analysis Date = 10/29/16 Pct Recovery = 97% Analysis Date = 10/29/16 Pct Recovery = 97% Analysis Date = 10/19/16 Pct Recovery = 97% Analysis Date = 10/19/16 Pct Recovery = 97% Analysis Date = 10/09/16 Pct Recovery = 97% Analysis Date = 10/09/16 Pct Recovery = 97% Analysis Date = 09/29/16 Pct Recovery = 97% Analysis Date = 09/29/16 Pct Recovery = 97% Analysis Date = 09/19/16 Pct Recovery = 97% Analysis Date = 09/19/16 Pct Recovery = 97% Analysis Date = 09/10/16 Pct Recovery = 96% Analysis Date = 09/10/16 Pct Recovery = 96% Analysis Date = 08/31/16 Pct Recovery = 96% Analysis Date = 08/31/16 Pct Recovery = 96% Analysis Date = 08/21/16 Pct Recovery = 96% Analysis Date = 08/21/16 Pct Recovery = 96% Analysis Date = 08/11/16 Pct Recovery = 96% Analysis Date = 08/11/16 Pct Recovery = 96% Analysis Date = 08/01/16 Pct Recovery = 96% Analysis Date = 08/01/16 Pct Recovery = 96% Analysis Date = 07/23/16 Pct Recovery = 96% Analysis Date = 07/23/16 Pct Recovery = 96% Analysis Date = 07/13/16 Pct Recovery = 96% Analysis Date = 07/13/16 Pct Recovery = 96% Analysis Date = 07/03/16 Pct Recovery = 96% Analysis Date = 07/03/16 Pct Recovery = 96% Analysis Date = 06/23/16 Pct Recovery = 96% Analysis Date = 06/23/16 Pct Recovery = 96% Analysis Date = 06/13/16 Pct Recovery = 96% Analysis Date = 06/13/16 Pct Recovery = 96% Analysis Date = 06/04/16 Pct Recovery = 96% Analysis Date = 06/04/16 Pct Recovery = 96% Analysis Date = 05/25/16 Pct Recovery = 96% Analysis Date = 05/25/16 Pct Recovery = 96% Analysis Date = 05/15/16 Pct Recovery = 96% Analysis Date = 05/15/16 Pct Recovery = 96% Analysis Date = 05/05/16 Pct Recovery = 96% Analysis Date = 05/05/16 Pct Recovery = 96% Analysis Date = 04/25/16 Pct Recovery = 96% Analysis Date = 04/25/16 Pct Recovery = 96% Analysis Date = 04/16/16 Pct Recovery = 96% Analysis Date = 04/16/16 Pct Recovery = 96% Analysis Date = 04/06/16 Pct Recovery = 96% Analysis Date = 04/06/16 Pct Recovery = 96% Analysis Date = 03/27/16 Pct Recovery = 96% Analysis Date = 03/27/16 Pct Recovery = 96% Analysis Date = 03/17/16 Pct Recovery = 96% Analysis Date = 03/17/16 Pct Recovery = 96% Analysis Date = 03/07/16 Pct Recovery = 96% Analysis Date = 03/07/16 Pct Recovery = 96% Analysis Date = 02/26/16 Pct Recovery = 96% Analysis Date = 02/26/16 Pct Recovery = 96% Analysis Date = 02/17/16 Pct Recovery = 96% Analysis Date = 02/17/16 Pct Recovery = 96% Analysis Date = 02/07/16 Pct Recovery = 96% Analysis Date = 02/07/16 Pct Recovery = 96% Analysis Date = 01/28/16 Pct Recovery = 96% Analysis Date = 01/28/16 Pct Recovery = 96% Analysis Date = 01/18/16 Pct Recovery = 96% Analysis Date = 01/18/16 Pct Recovery = 96% Analysis Date = 01/08/16 Pct Recovery = 96% Analysis Date = 01/08/16 Pct Recovery = 96% Analysis Date = 12/30/15 Pct Recovery = 96% Analysis Date = 12/30/15 Pct Recovery = 96% Analysis Date = 12/20/15 Pct Recovery = 96% Analysis Date = 12/20/15 Pct Recovery = 96% Analysis Date = 12/10/15 Pct Recovery = 96% Analysis Date = 12/10/15 Pct Recovery = 96% Analysis Date = 11/30/15 Pct Recovery = 96% Analysis Date = 11/30/15 Pct Recovery = 96% Analysis Date = 11/20/15 Pct Recovery = 96% Analysis Date = 11/20/15 Pct Recovery = 96% Analysis Date = 11/11/15 Pct Recovery = 96% Analysis Date = 11/11/15 Pct Recovery = 96% Analysis Date = 11/01/15 Pct Recovery = 97% Analysis Date = 11/01/15 Pct Recovery = 97% Analysis Date = 10/22/15 Pct Recovery = 97% Analysis Date = 10/22/15 Pct Recovery = 97% Analysis Date = 10/12/15 Pct Recovery = 97% Analysis Date = 10/12/15 Pct Recovery = 97% Analysis Date = 10/02/15 Pct Recovery = 97% Analysis Date = 10/02/15 Pct Recovery = 97% Analysis Date = 09/23/15 Pct Recovery = 97% Analysis Date = 09/23/15 Pct Recovery = 97% Analysis Date = 09/13/15 Pct Recovery = 97% Analysis Date = 09/13/15 Pct Recovery = 97% Analysis Date = 09/03/15 Pct Recovery = 97% Analysis Date = 09/03/15 Pct Recovery = 97% Analysis Date = 08/24/15 Pct Recovery = 97% Analysis Date = 08/24/15 Pct Recovery = 97% Analysis Date = 08/14/15 Pct Recovery = 97% Analysis Date = 08/14/15 Pct Recovery = 97% Analysis Date = 08/04/15 Pct Recovery = 97% Analysis Date = 08/04/15 Pct Recovery = 97% Analysis Date = 07/26/15 Pct Recovery = 97% Analysis Date = 07/26/15 Pct Recovery = 97% Analysis Date = 07/16/15 Pct Recovery = 97% Analysis Date = 07/16/15 Pct Recovery = 97% Analysis Date = 07/06/15 Pct Recovery = 97% Analysis Date = 07/06/15 Pct Recovery = 97% Analysis Date = 06/26/15 Pct Recovery = 98% Analysis Date = 06/26/15 Pct Recovery = 98% Analysis Date = 06/16/15 Pct Recovery = 98% Analysis Date = 06/16/15 Pct Recovery = 98% Analysis Date = 06/07/15 Pct Recovery = 98% Analysis Date = 06/07/15 Pct Recovery = 98% Analysis Date = 05/28/15 Pct Recovery = 98% Analysis Date = 05/28/15 Pct Recovery = 98% Analysis Date = 05/18/15 Pct Recovery = 98% Analysis Date = 05/18/15 Pct Recovery = 98% Analysis Date = 05/08/15 Pct Recovery = 98% Analysis Date = 05/08/15 Pct Recovery = 98% Analysis Date = 04/28/15 Pct Recovery = 98% Analysis Date = 04/28/15 Pct Recovery = 98% Analysis Date = 04/19/15 Pct Recovery = 98% Analysis Date = 04/19/15 Pct Recovery = 98% Analysis Date = 04/09/15 Pct Recovery = 98% Analysis Date = 04/09/15 Pct Recovery = 98% Analysis Date = 03/30/15 Pct Recovery = 98% Analysis Date = 03/30/15 Pct Recovery = 98% Analysis Date = 03/20/15 Pct Recovery = 99% Analysis Date = 03/20/15 Pct Recovery = 99% Analysis Date = 03/10/15 Pct Recovery = 99% Analysis Date = 03/10/15 Pct Recovery = 99% Analysis Date = 02/28/15 Pct Recovery = 99% Analysis Date = 02/28/15 Pct Recovery = 99% Analysis Date = 02/19/15 Pct Recovery = 99% Analysis Date = 02/19/15 Pct Recovery = 99% Analysis Date = 02/09/15 Pct Recovery = 99% Analysis Date = 02/09/15 Pct Recovery = 99% Analysis Date = 01/30/15 Pct Recovery = 99% Analysis Date = 01/30/15 Pct Recovery = 99% Analysis Date = 01/20/15 Pct Recovery = 99% Analysis Date = 01/20/15 Pct Recovery = 99% Analysis Date = 01/10/15 Pct Recovery = 99% Analysis Date = 01/10/15 Pct Recovery = 99% Analysis Date = 01/01/15 Pct Recovery = 99% Analysis Date = 01/01/15 Pct Recovery = 99% Analysis Date = 12/22/14 Pct Recovery = 99% Analysis Date = 12/22/14 Pct Recovery = 99% Analysis Date = 12/12/14 Pct Recovery = 100% Analysis Date = 12/12/14 Pct Recovery = 100% Analysis Date = 12/02/14 Pct Recovery = 100% Analysis Date = 12/02/14 Pct Recovery = 100% Analysis Date = 11/22/14 Pct Recovery = 100% Analysis Date = 11/22/14 Pct Recovery = 100% Analysis Date = 11/13/14 Pct Recovery = 100% Analysis Date = 11/13/14 Pct Recovery = 100% Analysis Date = 11/03/14 Pct Recovery = 100% Analysis Date = 11/03/14 Pct Recovery = 100% Analysis Date = 10/24/14 Pct Recovery = 100% Analysis Date = 10/24/14 Pct Recovery = 100% Analysis Date = 10/14/14 Pct Recovery = 100% Analysis Date = 10/14/14 Pct Recovery = 100% Analysis Date = 10/04/14 Pct Recovery = 100% Analysis Date = 10/04/14 Pct Recovery = 100% Analysis Date = 09/25/14 Pct Recovery = 100% Analysis Date = 09/25/14 Pct Recovery = 100% Analysis Date = 09/15/14 Pct Recovery = 100% Analysis Date = 09/15/14 Pct Recovery = 100% Analysis Date = 09/05/14 Pct Recovery = 101% Analysis Date = 09/05/14 Pct Recovery = 101% Analysis Date = 08/26/14 Pct Recovery = 101% Analysis Date = 08/26/14 Pct Recovery = 101% Analysis Date = 08/16/14 Pct Recovery = 101% Analysis Date = 08/16/14 Pct Recovery = 101% Analysis Date = 08/06/14 Pct Recovery = 101% Analysis Date = 08/06/14 Pct Recovery = 101% Analysis Date = 07/28/14 Pct Recovery = 101% Analysis Date = 07/28/14 Pct Recovery = 101% Analysis Date = 07/18/14 Pct Recovery = 101% Analysis Date = 07/18/14 Pct Recovery = 101% Analysis Date = 07/08/14 Pct Recovery = 102% Analysis Date = 07/08/14 Pct Recovery = 102% Analysis Date = 06/28/14 Pct Recovery = 102% Analysis Date = 06/28/14 Pct Recovery = 102% Analysis Date = 06/18/14 Pct Recovery = 102% Analysis Date = 06/18/14 Pct Recovery = 102% Analysis Date = 06/09/14 Pct Recovery = 102% Analysis Date = 06/09/14 Pct Recovery = 102% Analysis Date = 05/30/14 Pct Recovery = 102% Analysis Date = 05/30/14 Pct Recovery = 102% Analysis Date = 05/20/14 Pct Recovery = 102% Analysis Date = 05/20/14 Pct Recovery = 102% Analysis Date = 05/10/14 Pct Recovery = 102% Analysis Date = 05/10/14 Pct Recovery = 102% Analysis Date = 04/30/14 Pct Recovery = 102% Analysis Date = 04/30/14 Pct Recovery = 102% Analysis Date = 04/21/14 Pct Recovery = 102% Analysis Date = 04/21/14 Pct Recovery = 102% Analysis Date = 04/11/14 Pct Recovery = 103% Analysis Date = 04/11/14 Pct Recovery = 103% Analysis Date = 04/01/14 Pct Recovery = 103% Analysis Date = 04/01/14 Pct Recovery = 103% Analysis Date = 03/22/14 Pct Recovery = 103% Analysis Date = 03/22/14 Pct Recovery = 103% Analysis Date = 03/12/14 Pct Recovery = 103% Analysis Date = 03/12/14 Pct Recovery = 103% Analysis Date = 03/03/14 Pct Recovery = 103% Analysis Date = 03/03/14 Pct Recovery = 103% Analysis Date = 02/21/14 Pct Recovery = 103% Analysis Date = 02/21/14 Pct Recovery = 103% Analysis Date = 02/11/14 Pct Recovery = 103% Analysis Date = 02/11/14 Pct Recovery = 103% Analysis Date = 02/01/14 Pct Recovery = 103% Analysis Date = 02/01/14 Pct Recovery = 103% Analysis Date = 01/22/14 Pct Recovery = 103% Analysis Date = 01/22/14 Pct Recovery = 103% Analysis Date = 01/12/14 Pct Recovery = 103% Analysis Date = 01/12/14 Pct Recovery = 103% Analysis Date = 01/03/14 Pct Recovery = 103% Analysis Date = 01/03/14 Pct Recovery = 103% Analysis Date = 12/24/13 Pct Recovery = 103% Analysis Date = 12/24/13 Pct Recovery = 103% Analysis Date = 12/14/13 Pct Recovery = 104% Analysis Date = 12/14/13 Pct Recovery = 104% Analysis Date = 12/04/13 Pct Recovery = 104% Analysis Date = 12/04/13 Pct Recovery = 104% Analysis Date = 11/24/13 Pct Recovery = 104% Analysis Date = 11/24/13 Pct Recovery = 104% Analysis Date = 11/15/13 Pct Recovery = 104% Analysis Date = 11/15/13 Pct Recovery = 104% Analysis Date = 11/05/13 Pct Recovery = 104% Analysis Date = 11/05/13 Pct Recovery = 104% Analysis Date = 10/26/13 Pct Recovery = 104% Analysis Date = 10/26/13 Pct Recovery = 104% Analysis Date = 10/16/13 Pct Recovery = 104% Analysis Date = 10/16/13 Pct Recovery = 104% Analysis Date = 10/06/13 Pct Recovery = 104% Analysis Date = 10/06/13 Pct Recovery = 104% Analysis Date = 09/27/13 Pct Recovery = 104% Analysis Date = 09/27/13 Pct Recovery = 104% Analysis Date = 09/17/13 Pct Recovery = 104% Analysis Date = 09/17/13 Pct Recovery = 104% Analysis Date = 09/07/13 Pct Recovery = 104% Analysis Date = 09/07/13 Pct Recovery = 104% Analysis Date = 08/28/13 Pct Recovery = 104% Analysis Date = 08/28/13 Pct Recovery = 104% Analysis Date = 08/18/13 Pct Recovery = 104% Analysis Date = 08/18/13 Pct Recovery = 104% Analysis Date = 08/09/13 Pct Recovery = 104% Analysis Date = 08/09/13 Pct Recovery = 104% Analysis Date = 07/30/13 Pct Recovery = 104% Analysis Date = 07/30/13 Pct Recovery = 104% Analysis Date = 07/20/13 Pct Recovery = 104% Analysis Date = 07/20/13 Pct Recovery = 104% Analysis Date = 07/10/13 Pct Recovery = 105% Analysis Date = 07/10/13 Pct Recovery = 105% Analysis Date = 06/30/13 Pct Recovery = 105% Analysis Date = 06/30/13 Pct Recovery = 105% Analysis Date = 06/20/13 Pct Recovery = 105% Analysis Date = 06/20/13 Pct Recovery = 105% Analysis Date = 06/11/13 Pct Recovery = 105% Analysis Date = 06/11/13 Pct Recovery = 105% Analysis Date = 06/01/13 Pct Recovery = 105% Analysis Date = 06/01/13 Pct Recovery = 105% Analysis Date = 05/22/13 Pct Recovery = 105% Analysis Date = 05/22/13 Pct Recovery = 105% Analysis Date = 05/12/13 Pct Recovery = 105% Analysis Date = 05/12/13 Pct Recovery = 105% Analysis Date = 05/02/13 Pct Recovery = 105% Analysis Date = 05/02/13 Pct Recovery = 105% Analysis Date = 04/23/13 Pct Recovery = 105% Analysis Date = 04/23/13 Pct Recovery = 105% Analysis Date = 04/13/13 Pct Recovery = 105% Analysis Date = 04/13/13 Pct Recovery = 105% Analysis Date = 04/03/13 Pct Recovery = 105% Analysis Date = 04/03/13 Pct Recovery = 105% Analysis Date = 03/24/13 Pct Recovery = 105% Analysis Date = 03/24/13 Pct Recovery = 105% Analysis Date = 03/14/13 Pct Recovery = 105% Analysis Date = 03/14/13 Pct Recovery = 105% Analysis Date = 03/05/13 Pct Recovery = 105% Analysis Date = 03/05/13 Pct Recovery = 105% Analysis Date = 02/23/13 Pct Recovery = 105% Analysis Date = 02/23/13 Pct Recovery = 105% Analysis Date = 02/13/13 Pct Recovery = 105% Analysis Date = 02/13/13 Pct Recovery = 105% Analysis Date = 02/03/13 Pct Recovery = 105% Analysis Date = 02/03/13 Pct Recovery = 105% Analysis Date = 01/24/13 Pct Recovery = 105% Analysis Date = 01/24/13 Pct Recovery = 105% Analysis Date = 01/15/13 Pct Recovery = 105% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
DACTHAL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 84 100% 12% 98% 10%
Total 84 100% 12% 98% 10%

Sample Statistics
DACTHAL

Characteristic N % % Basis
Plotted 84 100% Spiked
Estimated Values 2 2% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 84 .  
False Negatives 0 0% 0 out of 84
Not Spiked 50 .  
False Positives 0 0% 0 out of 50

OBSP Determination:
DEETHYLATRAZINE
METHOD: 2033 , TESTIDCODE: 04040GCM35

Laboratory ID = 20140100085 Lab Value = 0.081 Expected Conc. = 0.22 Report level label = 0.01 Pct Recovery = 37% Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl SpecificMix = T1130514013 Laboratory ID = 20132490342 Lab Value = 0.094 Expected Conc. = 0.22 Report level label = 0.01 Pct Recovery = 43% Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl SpecificMix = T1130514013 Laboratory ID = 20131370001 Lab Value = 0.077 Expected Conc. = 0.113 Report level label = 0.01 Pct Recovery = 68% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl SpecificMix = 1473000 Laboratory ID = 20140370077 Lab Value = 0.040 Expected Conc. = 0.11 Report level label = 0.01 Pct Recovery = 36% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl SpecificMix = T1130514013 Laboratory ID = 20132690010 Lab Value = 0.071 Expected Conc. = 0.11 Report level label = 0.01 Pct Recovery = 65% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl SpecificMix = T1130514013 Laboratory ID = 20130250061 Lab Value = 0.028 Expected Conc. = 0.1 Report level label = 0.01 Pct Recovery = 28% Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl SpecificMix = A088380 Laboratory ID = 20163370001 Lab Value = 0.032 Expected Conc. = 0.0625 Report level label = 0.01 Pct Recovery = 51% Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl SpecificMix = LC20138V Laboratory ID = 20162860079 Lab Value = 0.033 Expected Conc. = 0.06 Report level label = 0.01 Pct Recovery = 55% Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl SpecificMix = 5054800 Laboratory ID = 20161880109 Lab Value = 0.031 Expected Conc. = 0.06 Report level label = 0.01 Pct Recovery = 52% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl SpecificMix = 5054800 Laboratory ID = 20152750006 Lab Value = 0.020 Expected Conc. = 0.06 Report level label = 0.01 Pct Recovery = 33% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl SpecificMix = EN150514012 Laboratory ID = 20152460215 Lab Value = 0.023 Expected Conc. = 0.06 Report level label = 0.01 Pct Recovery = 38% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl SpecificMix = EN150514012 Laboratory ID = 20171720140 Lab Value = 0.020 Expected Conc. = 0.05 Report level label = 0.01 Pct Recovery = 40% Analysis Date = 08/31/17 SpikeMix = Supelco LC20138V: 80 µl & Phenova B20160331: 80 µl SpecificMix = LC20138V Laboratory ID = 20170740063 Lab Value = 0.006 Expected Conc. = 0.05 Report level label = 0.01 Pct Recovery = 11% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl SpecificMix = LC20138V Laboratory ID = 20161470001 Lab Value = 0.025 Expected Conc. = 0.05 Report level label = 0.01 Pct Recovery = 50% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl SpecificMix = LC20138V Laboratory ID = 20140230082 Lab Value = 0.019 Expected Conc. = 0.05 Report level label = 0.01 Pct Recovery = 38% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl SpecificMix = A093651 Laboratory ID = 20132420001 Lab Value = 0.024 Expected Conc. = 0.05 Report level label = 0.01 Pct Recovery = 47% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl SpecificMix = A093651 Laboratory ID = 20130810108 Lab Value = 0.029 Expected Conc. = 0.05 Report level label = 0.01 Pct Recovery = 57% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl SpecificMix = T1120530013 Laboratory ID = 20123560092 Lab Value = 0.027 Expected Conc. = 0.05 Report level label = 0.01 Pct Recovery = 55% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = T1120530013 Laboratory ID = 20171380001 Lab Value = 0.017 Expected Conc. = 0.048 Report level label = 0.01 Pct Recovery = 36% Analysis Date = 06/07/17 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 5054800 Laboratory ID = 20170960001 Lab Value = 0.023 Expected Conc. = 0.048 Report level label = 0.01 Pct Recovery = 49% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl SpecificMix = 5054800 Laboratory ID = 20161740258 Lab Value = 0.016 Expected Conc. = 0.048 Report level label = 0.01 Pct Recovery = 33% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 5054800 Laboratory ID = 20140730138 Lab Value = 0.008 Expected Conc. = 0.0452 Report level label = 0.01 Pct Recovery = 17% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 1473000 Laboratory ID = 20133470008 Lab Value = 0.028 Expected Conc. = 0.0452 Report level label = 0.01 Pct Recovery = 62% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl SpecificMix = 1473000 Laboratory ID = 20133310030 Lab Value = 0.023 Expected Conc. = 0.0452 Report level label = 0.01 Pct Recovery = 51% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl SpecificMix = 1473000 Laboratory ID = 20131790009 Lab Value = 0.037 Expected Conc. = 0.0452 Report level label = 0.01 Pct Recovery = 83% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl SpecificMix = 1473000 Laboratory ID = 20131650073 Lab Value = 0.037 Expected Conc. = 0.0452 Report level label = 0.01 Pct Recovery = 81% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl SpecificMix = 1473000 Laboratory ID = 20133050050 Lab Value = 0.026 Expected Conc. = 0.044 Report level label = 0.01 Pct Recovery = 60% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl SpecificMix = T1130514013 Laboratory ID = 20132280016 Lab Value = 0.038 Expected Conc. = 0.044 Report level label = 0.01 Pct Recovery = 85% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl SpecificMix = T1130514013 Laboratory ID = 20150720069 Lab Value = 0.006 Expected Conc. = 0.0402 Report level label = 0.01 Pct Recovery = 16% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 03DD006 Laboratory ID = 20143110108 Lab Value = 0.015 Expected Conc. = 0.0402 Report level label = 0.01 Pct Recovery = 37% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 03DD006 Laboratory ID = 20142960086 Lab Value = 0.015 Expected Conc. = 0.0402 Report level label = 0.01 Pct Recovery = 38% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 03DD006 Laboratory ID = 20142720002 Lab Value = 0.014 Expected Conc. = 0.0402 Report level label = 0.01 Pct Recovery = 35% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl SpecificMix = LC06435 Laboratory ID = 20142530087 Lab Value = 0.013 Expected Conc. = 0.0402 Report level label = 0.01 Pct Recovery = 32% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl SpecificMix = LC06435 Laboratory ID = 20142270001 Lab Value = 0.014 Expected Conc. = 0.0402 Report level label = 0.01 Pct Recovery = 36% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl SpecificMix = 03DD006 Laboratory ID = 20141570088 Lab Value = 0.020 Expected Conc. = 0.0402 Report level label = 0.01 Pct Recovery = 49% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl SpecificMix = LC06435 Laboratory ID = 20141220025 Lab Value = 0.023 Expected Conc. = 0.0402 Report level label = 0.01 Pct Recovery = 56% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl SpecificMix = LC06435 Laboratory ID = 20172230001 Lab Value = 0.023 Expected Conc. = 0.035 Report level label = 0.01 Pct Recovery = 66% Analysis Date = 10/19/17 SpikeMix = ChemService 6472100: 50 µl & Abs 071717Pest: 50 µl SpecificMix = 6472100 Laboratory ID = 20172560101 Lab Value = 0.016 Expected Conc. = 0.0337 Report level label = 0.01 Pct Recovery = 48% Analysis Date = 12/22/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6567600: 50 µl SpecificMix = EN170808006 Laboratory ID = 20172370001 Lab Value = 0.017 Expected Conc. = 0.0337 Report level label = 0.01 Pct Recovery = 51% Analysis Date = 11/18/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6537100: 50 µl SpecificMix = EN170808006 Laboratory ID = 20160630046 Lab Value = 0.014 Expected Conc. = 0.03 Report level label = 0.01 Pct Recovery = 47% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = EN150514012 Laboratory ID = 20153440001 Lab Value = 0.013 Expected Conc. = 0.03 Report level label = 0.01 Pct Recovery = 44% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = EN150514012 Laboratory ID = 20152330039 Lab Value = 0.015 Expected Conc. = 0.03 Report level label = 0.01 Pct Recovery = 50% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl SpecificMix = 041415 Laboratory ID = 20151900132 Lab Value = 0.015 Expected Conc. = 0.03 Report level label = 0.01 Pct Recovery = 51% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl SpecificMix = 041415 Laboratory ID = 20151270112 Lab Value = 0.015 Expected Conc. = 0.03 Report level label = 0.01 Pct Recovery = 50% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl SpecificMix = 041415 Laboratory ID = 20171510080 Lab Value = 0.017 Expected Conc. = 0.025 Report level label = 0.01 Pct Recovery = 69% Analysis Date = 06/09/17 SpikeMix = Supelco LC20138V: 40 µl & Crescent 03FF076: 40 µl SpecificMix = LC20138V Laboratory ID = 20162520001 Lab Value = 0.018 Expected Conc. = 0.025 Report level label = 0.01 Pct Recovery = 70% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl SpecificMix = LC20138V Laboratory ID = 20162660005 Lab Value = 0.014 Expected Conc. = 0.025 Report level label = 0.01 Pct Recovery = 58% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl SpecificMix = LC20138V Laboratory ID = 20162020124 Lab Value = 0.016 Expected Conc. = 0.025 Report level label = 0.01 Pct Recovery = 62% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl SpecificMix = LC20138V Laboratory ID = 20171940002 Lab Value = 0.016 Expected Conc. = 0.024 Report level label = 0.01 Pct Recovery = 67% Analysis Date = 11/10/17 SpikeMix = ChemService 5054800: 40 µl & NSI 041816: 40 µl SpecificMix = 5054800 Laboratory ID = 20170460061 Lab Value = 0.013 Expected Conc. = 0.024 Report level label = 0.01 Pct Recovery = 55% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl SpecificMix = 5054800 Laboratory ID = 20163560019 Lab Value = 0.013 Expected Conc. = 0.024 Report level label = 0.01 Pct Recovery = 55% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl SpecificMix = 5054800 Laboratory ID = 20162150213 Lab Value = 0.013 Expected Conc. = 0.024 Report level label = 0.01 Pct Recovery = 56% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl SpecificMix = 5054800 Laboratory ID = 20173120093 Lab Value = 0.016 Expected Conc. = 0.021 Report level label = 0.01 Pct Recovery = 77% Analysis Date = 03/10/18 SpikeMix = ChemService 6472100: 30 µl & ChemService 6537100: 30 µl SpecificMix = 6472100 Laboratory ID = 20150150115 Lab Value = 0.011 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 55% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl SpecificMix = LC06435 Laboratory ID = 20143370094 Lab Value = 0.010 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 52% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl SpecificMix = LC06435 Laboratory ID = 20142200164 Lab Value = 0.010 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 52% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 03DD006 Laboratory ID = 20141910243 Lab Value = 0.011 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 54% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = LC06435 Laboratory ID = 20141840097 Lab Value = 0.010 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 50% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl SpecificMix = LC06435 Laboratory ID = 20141640076 Lab Value = 0.010 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 51% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = 03DD006 Laboratory ID = 20141420140 Lab Value = 0.007 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 37% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 03DD006 Laboratory ID = 20141080004 Lab Value = 0.010 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 51% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl SpecificMix = 03DD006 Laboratory ID = 20140860102 Lab Value = 0.013 Expected Conc. = 0.02 Report level label = 0.01 Pct Recovery = 63% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl SpecificMix = A093651 Laboratory ID = 20133400002 Lab Value = 0.013 Expected Conc. = 0.02 Report level label = 0.01 Pct Recovery = 63% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = A093651 Laboratory ID = 20132910008 Lab Value = 0.012 Expected Conc. = 0.02 Report level label = 0.01 Pct Recovery = 58% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = A093651 Laboratory ID = 20131920149 Lab Value = 0.016 Expected Conc. = 0.02 Report level label = 0.01 Pct Recovery = 80% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl SpecificMix = A093651 Laboratory ID = 20131230084 Lab Value = 0.016 Expected Conc. = 0.02 Report level label = 0.01 Pct Recovery = 78% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl SpecificMix = A088380 Laboratory ID = 20130650005 Lab Value = 0.010 Expected Conc. = 0.02 Report level label = 0.01 Pct Recovery = 51% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl SpecificMix = A088380 Laboratory ID = 20130390105 Lab Value = 0.012 Expected Conc. = 0.02 Report level label = 0.01 Pct Recovery = 58% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl SpecificMix = T1120530013 Laboratory ID = 20161050143 Lab Value = 0.010 Expected Conc. = 0.015 Report level label = 0.01 Pct Recovery = 69% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 041415 Laboratory ID = 20160560044 Lab Value = 0.010 Expected Conc. = 0.015 Report level label = 0.01 Pct Recovery = 64% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl SpecificMix = 041415 Laboratory ID = 20160210080 Lab Value = 0.009 Expected Conc. = 0.015 Report level label = 0.01 Pct Recovery = 61% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 041415 Laboratory ID = 20160070059 Lab Value = 0.008 Expected Conc. = 0.015 Report level label = 0.01 Pct Recovery = 54% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = EN150514012 Laboratory ID = 20153160001 Lab Value = 0.010 Expected Conc. = 0.015 Report level label = 0.01 Pct Recovery = 69% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = EN150514012 Laboratory ID = 20152950078 Lab Value = 0.008 Expected Conc. = 0.015 Report level label = 0.01 Pct Recovery = 52% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 041415 Laboratory ID = 20152040177 Lab Value = 0.010 Expected Conc. = 0.015 Report level label = 0.01 Pct Recovery = 64% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl SpecificMix = 041415 Laboratory ID = 20151760208 Lab Value = 0.009 Expected Conc. = 0.015 Report level label = 0.01 Pct Recovery = 58% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl SpecificMix = EN150514012 Laboratory ID = 20151480170 Lab Value = 0.010 Expected Conc. = 0.015 Report level label = 0.01 Pct Recovery = 69% Analysis Date = 06/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150514012 Laboratory ID = 20151210037 Lab Value = 0.011 Expected Conc. = 0.015 Report level label = 0.01 Pct Recovery = 73% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 041415 Analysis Date = 03/10/18 Pct Recovery = 56% Analysis Date = 02/28/18 Pct Recovery = 56% Analysis Date = 02/28/18 Pct Recovery = 56% Analysis Date = 02/19/18 Pct Recovery = 56% Analysis Date = 02/19/18 Pct Recovery = 56% Analysis Date = 02/09/18 Pct Recovery = 56% Analysis Date = 02/09/18 Pct Recovery = 56% Analysis Date = 01/31/18 Pct Recovery = 56% Analysis Date = 01/31/18 Pct Recovery = 56% Analysis Date = 01/22/18 Pct Recovery = 56% Analysis Date = 01/22/18 Pct Recovery = 56% Analysis Date = 01/12/18 Pct Recovery = 55% Analysis Date = 01/12/18 Pct Recovery = 55% Analysis Date = 01/03/18 Pct Recovery = 55% Analysis Date = 01/03/18 Pct Recovery = 55% Analysis Date = 12/24/17 Pct Recovery = 55% Analysis Date = 12/24/17 Pct Recovery = 55% Analysis Date = 12/15/17 Pct Recovery = 55% Analysis Date = 12/15/17 Pct Recovery = 55% Analysis Date = 12/06/17 Pct Recovery = 55% Analysis Date = 12/06/17 Pct Recovery = 55% Analysis Date = 11/26/17 Pct Recovery = 55% Analysis Date = 11/26/17 Pct Recovery = 55% Analysis Date = 11/17/17 Pct Recovery = 55% Analysis Date = 11/17/17 Pct Recovery = 55% Analysis Date = 11/07/17 Pct Recovery = 55% Analysis Date = 11/07/17 Pct Recovery = 55% Analysis Date = 10/29/17 Pct Recovery = 55% Analysis Date = 10/29/17 Pct Recovery = 55% Analysis Date = 10/20/17 Pct Recovery = 55% Analysis Date = 10/20/17 Pct Recovery = 55% Analysis Date = 10/10/17 Pct Recovery = 55% Analysis Date = 10/10/17 Pct Recovery = 55% Analysis Date = 10/01/17 Pct Recovery = 55% Analysis Date = 10/01/17 Pct Recovery = 55% Analysis Date = 09/21/17 Pct Recovery = 55% Analysis Date = 09/21/17 Pct Recovery = 55% Analysis Date = 09/12/17 Pct Recovery = 55% Analysis Date = 09/12/17 Pct Recovery = 55% Analysis Date = 09/03/17 Pct Recovery = 55% Analysis Date = 09/03/17 Pct Recovery = 55% Analysis Date = 08/24/17 Pct Recovery = 55% Analysis Date = 08/24/17 Pct Recovery = 55% Analysis Date = 08/15/17 Pct Recovery = 55% Analysis Date = 08/15/17 Pct Recovery = 55% Analysis Date = 08/05/17 Pct Recovery = 55% Analysis Date = 08/05/17 Pct Recovery = 55% Analysis Date = 07/27/17 Pct Recovery = 54% Analysis Date = 07/27/17 Pct Recovery = 54% Analysis Date = 07/18/17 Pct Recovery = 54% Analysis Date = 07/18/17 Pct Recovery = 54% Analysis Date = 07/08/17 Pct Recovery = 54% Analysis Date = 07/08/17 Pct Recovery = 54% Analysis Date = 06/29/17 Pct Recovery = 54% Analysis Date = 06/29/17 Pct Recovery = 54% Analysis Date = 06/19/17 Pct Recovery = 54% Analysis Date = 06/19/17 Pct Recovery = 54% Analysis Date = 06/10/17 Pct Recovery = 54% Analysis Date = 06/10/17 Pct Recovery = 54% Analysis Date = 06/01/17 Pct Recovery = 54% Analysis Date = 06/01/17 Pct Recovery = 54% Analysis Date = 05/22/17 Pct Recovery = 54% Analysis Date = 05/22/17 Pct Recovery = 54% Analysis Date = 05/13/17 Pct Recovery = 54% Analysis Date = 05/13/17 Pct Recovery = 54% Analysis Date = 05/03/17 Pct Recovery = 54% Analysis Date = 05/03/17 Pct Recovery = 54% Analysis Date = 04/24/17 Pct Recovery = 54% Analysis Date = 04/24/17 Pct Recovery = 54% Analysis Date = 04/15/17 Pct Recovery = 54% Analysis Date = 04/15/17 Pct Recovery = 54% Analysis Date = 04/05/17 Pct Recovery = 54% Analysis Date = 04/05/17 Pct Recovery = 54% Analysis Date = 03/27/17 Pct Recovery = 54% Analysis Date = 03/27/17 Pct Recovery = 54% Analysis Date = 03/17/17 Pct Recovery = 54% Analysis Date = 03/17/17 Pct Recovery = 54% Analysis Date = 03/08/17 Pct Recovery = 54% Analysis Date = 03/08/17 Pct Recovery = 54% Analysis Date = 02/27/17 Pct Recovery = 54% Analysis Date = 02/27/17 Pct Recovery = 54% Analysis Date = 02/17/17 Pct Recovery = 54% Analysis Date = 02/17/17 Pct Recovery = 54% Analysis Date = 02/08/17 Pct Recovery = 53% Analysis Date = 02/08/17 Pct Recovery = 53% Analysis Date = 01/29/17 Pct Recovery = 53% Analysis Date = 01/29/17 Pct Recovery = 53% Analysis Date = 01/20/17 Pct Recovery = 53% Analysis Date = 01/20/17 Pct Recovery = 53% Analysis Date = 01/11/17 Pct Recovery = 53% Analysis Date = 01/11/17 Pct Recovery = 53% Analysis Date = 01/01/17 Pct Recovery = 53% Analysis Date = 01/01/17 Pct Recovery = 53% Analysis Date = 12/23/16 Pct Recovery = 53% Analysis Date = 12/23/16 Pct Recovery = 53% Analysis Date = 12/13/16 Pct Recovery = 53% Analysis Date = 12/13/16 Pct Recovery = 53% Analysis Date = 12/04/16 Pct Recovery = 53% Analysis Date = 12/04/16 Pct Recovery = 53% Analysis Date = 11/25/16 Pct Recovery = 53% Analysis Date = 11/25/16 Pct Recovery = 53% Analysis Date = 11/15/16 Pct Recovery = 53% Analysis Date = 11/15/16 Pct Recovery = 53% Analysis Date = 11/06/16 Pct Recovery = 53% Analysis Date = 11/06/16 Pct Recovery = 53% Analysis Date = 10/27/16 Pct Recovery = 53% Analysis Date = 10/27/16 Pct Recovery = 53% Analysis Date = 10/18/16 Pct Recovery = 53% Analysis Date = 10/18/16 Pct Recovery = 53% Analysis Date = 10/09/16 Pct Recovery = 53% Analysis Date = 10/09/16 Pct Recovery = 53% Analysis Date = 09/29/16 Pct Recovery = 53% Analysis Date = 09/29/16 Pct Recovery = 53% Analysis Date = 09/20/16 Pct Recovery = 53% Analysis Date = 09/20/16 Pct Recovery = 53% Analysis Date = 09/10/16 Pct Recovery = 53% Analysis Date = 09/10/16 Pct Recovery = 53% Analysis Date = 09/01/16 Pct Recovery = 53% Analysis Date = 09/01/16 Pct Recovery = 53% Analysis Date = 08/23/16 Pct Recovery = 53% Analysis Date = 08/23/16 Pct Recovery = 53% Analysis Date = 08/13/16 Pct Recovery = 53% Analysis Date = 08/13/16 Pct Recovery = 53% Analysis Date = 08/04/16 Pct Recovery = 53% Analysis Date = 08/04/16 Pct Recovery = 53% Analysis Date = 07/25/16 Pct Recovery = 53% Analysis Date = 07/25/16 Pct Recovery = 53% Analysis Date = 07/16/16 Pct Recovery = 53% Analysis Date = 07/16/16 Pct Recovery = 53% Analysis Date = 07/07/16 Pct Recovery = 53% Analysis Date = 07/07/16 Pct Recovery = 53% Analysis Date = 06/27/16 Pct Recovery = 53% Analysis Date = 06/27/16 Pct Recovery = 53% Analysis Date = 06/18/16 Pct Recovery = 53% Analysis Date = 06/18/16 Pct Recovery = 53% Analysis Date = 06/08/16 Pct Recovery = 53% Analysis Date = 06/08/16 Pct Recovery = 53% Analysis Date = 05/30/16 Pct Recovery = 53% Analysis Date = 05/30/16 Pct Recovery = 53% Analysis Date = 05/21/16 Pct Recovery = 53% Analysis Date = 05/21/16 Pct Recovery = 53% Analysis Date = 05/11/16 Pct Recovery = 53% Analysis Date = 05/11/16 Pct Recovery = 53% Analysis Date = 05/02/16 Pct Recovery = 53% Analysis Date = 05/02/16 Pct Recovery = 53% Analysis Date = 04/22/16 Pct Recovery = 53% Analysis Date = 04/22/16 Pct Recovery = 53% Analysis Date = 04/13/16 Pct Recovery = 53% Analysis Date = 04/13/16 Pct Recovery = 53% Analysis Date = 04/04/16 Pct Recovery = 53% Analysis Date = 04/04/16 Pct Recovery = 53% Analysis Date = 03/25/16 Pct Recovery = 53% Analysis Date = 03/25/16 Pct Recovery = 53% Analysis Date = 03/16/16 Pct Recovery = 53% Analysis Date = 03/16/16 Pct Recovery = 53% Analysis Date = 03/06/16 Pct Recovery = 53% Analysis Date = 03/06/16 Pct Recovery = 53% Analysis Date = 02/26/16 Pct Recovery = 53% Analysis Date = 02/26/16 Pct Recovery = 53% Analysis Date = 02/17/16 Pct Recovery = 53% Analysis Date = 02/17/16 Pct Recovery = 53% Analysis Date = 02/07/16 Pct Recovery = 53% Analysis Date = 02/07/16 Pct Recovery = 53% Analysis Date = 01/29/16 Pct Recovery = 53% Analysis Date = 01/29/16 Pct Recovery = 53% Analysis Date = 01/19/16 Pct Recovery = 53% Analysis Date = 01/19/16 Pct Recovery = 53% Analysis Date = 01/10/16 Pct Recovery = 53% Analysis Date = 01/10/16 Pct Recovery = 53% Analysis Date = 01/01/16 Pct Recovery = 52% Analysis Date = 01/01/16 Pct Recovery = 52% Analysis Date = 12/22/15 Pct Recovery = 52% Analysis Date = 12/22/15 Pct Recovery = 52% Analysis Date = 12/13/15 Pct Recovery = 52% Analysis Date = 12/13/15 Pct Recovery = 52% Analysis Date = 12/03/15 Pct Recovery = 52% Analysis Date = 12/03/15 Pct Recovery = 52% Analysis Date = 11/24/15 Pct Recovery = 52% Analysis Date = 11/24/15 Pct Recovery = 52% Analysis Date = 11/15/15 Pct Recovery = 52% Analysis Date = 11/15/15 Pct Recovery = 52% Analysis Date = 11/05/15 Pct Recovery = 52% Analysis Date = 11/05/15 Pct Recovery = 52% Analysis Date = 10/27/15 Pct Recovery = 52% Analysis Date = 10/27/15 Pct Recovery = 52% Analysis Date = 10/17/15 Pct Recovery = 52% Analysis Date = 10/17/15 Pct Recovery = 52% Analysis Date = 10/08/15 Pct Recovery = 51% Analysis Date = 10/08/15 Pct Recovery = 51% Analysis Date = 09/29/15 Pct Recovery = 51% Analysis Date = 09/29/15 Pct Recovery = 51% Analysis Date = 09/19/15 Pct Recovery = 51% Analysis Date = 09/19/15 Pct Recovery = 51% Analysis Date = 09/10/15 Pct Recovery = 51% Analysis Date = 09/10/15 Pct Recovery = 51% Analysis Date = 08/31/15 Pct Recovery = 51% Analysis Date = 08/31/15 Pct Recovery = 51% Analysis Date = 08/22/15 Pct Recovery = 51% Analysis Date = 08/22/15 Pct Recovery = 51% Analysis Date = 08/13/15 Pct Recovery = 51% Analysis Date = 08/13/15 Pct Recovery = 51% Analysis Date = 08/03/15 Pct Recovery = 51% Analysis Date = 08/03/15 Pct Recovery = 51% Analysis Date = 07/25/15 Pct Recovery = 51% Analysis Date = 07/25/15 Pct Recovery = 51% Analysis Date = 07/15/15 Pct Recovery = 50% Analysis Date = 07/15/15 Pct Recovery = 50% Analysis Date = 07/06/15 Pct Recovery = 50% Analysis Date = 07/06/15 Pct Recovery = 50% Analysis Date = 06/27/15 Pct Recovery = 50% Analysis Date = 06/27/15 Pct Recovery = 50% Analysis Date = 06/17/15 Pct Recovery = 50% Analysis Date = 06/17/15 Pct Recovery = 50% Analysis Date = 06/08/15 Pct Recovery = 50% Analysis Date = 06/08/15 Pct Recovery = 50% Analysis Date = 05/29/15 Pct Recovery = 50% Analysis Date = 05/29/15 Pct Recovery = 50% Analysis Date = 05/20/15 Pct Recovery = 50% Analysis Date = 05/20/15 Pct Recovery = 50% Analysis Date = 05/11/15 Pct Recovery = 50% Analysis Date = 05/11/15 Pct Recovery = 50% Analysis Date = 05/01/15 Pct Recovery = 49% Analysis Date = 05/01/15 Pct Recovery = 49% Analysis Date = 04/22/15 Pct Recovery = 49% Analysis Date = 04/22/15 Pct Recovery = 49% Analysis Date = 04/12/15 Pct Recovery = 49% Analysis Date = 04/12/15 Pct Recovery = 49% Analysis Date = 04/03/15 Pct Recovery = 49% Analysis Date = 04/03/15 Pct Recovery = 49% Analysis Date = 03/25/15 Pct Recovery = 49% Analysis Date = 03/25/15 Pct Recovery = 49% Analysis Date = 03/15/15 Pct Recovery = 49% Analysis Date = 03/15/15 Pct Recovery = 49% Analysis Date = 03/06/15 Pct Recovery = 49% Analysis Date = 03/06/15 Pct Recovery = 49% Analysis Date = 02/24/15 Pct Recovery = 49% Analysis Date = 02/24/15 Pct Recovery = 49% Analysis Date = 02/15/15 Pct Recovery = 48% Analysis Date = 02/15/15 Pct Recovery = 48% Analysis Date = 02/06/15 Pct Recovery = 48% Analysis Date = 02/06/15 Pct Recovery = 48% Analysis Date = 01/27/15 Pct Recovery = 48% Analysis Date = 01/27/15 Pct Recovery = 48% Analysis Date = 01/18/15 Pct Recovery = 48% Analysis Date = 01/18/15 Pct Recovery = 48% Analysis Date = 01/08/15 Pct Recovery = 48% Analysis Date = 01/08/15 Pct Recovery = 48% Analysis Date = 12/30/14 Pct Recovery = 48% Analysis Date = 12/30/14 Pct Recovery = 48% Analysis Date = 12/21/14 Pct Recovery = 48% Analysis Date = 12/21/14 Pct Recovery = 48% Analysis Date = 12/11/14 Pct Recovery = 48% Analysis Date = 12/11/14 Pct Recovery = 48% Analysis Date = 12/02/14 Pct Recovery = 48% Analysis Date = 12/02/14 Pct Recovery = 48% Analysis Date = 11/22/14 Pct Recovery = 48% Analysis Date = 11/22/14 Pct Recovery = 48% Analysis Date = 11/13/14 Pct Recovery = 48% Analysis Date = 11/13/14 Pct Recovery = 48% Analysis Date = 11/04/14 Pct Recovery = 48% Analysis Date = 11/04/14 Pct Recovery = 48% Analysis Date = 10/25/14 Pct Recovery = 48% Analysis Date = 10/25/14 Pct Recovery = 48% Analysis Date = 10/16/14 Pct Recovery = 48% Analysis Date = 10/16/14 Pct Recovery = 48% Analysis Date = 10/06/14 Pct Recovery = 48% Analysis Date = 10/06/14 Pct Recovery = 48% Analysis Date = 09/27/14 Pct Recovery = 48% Analysis Date = 09/27/14 Pct Recovery = 48% Analysis Date = 09/18/14 Pct Recovery = 48% Analysis Date = 09/18/14 Pct Recovery = 48% Analysis Date = 09/08/14 Pct Recovery = 48% Analysis Date = 09/08/14 Pct Recovery = 48% Analysis Date = 08/30/14 Pct Recovery = 48% Analysis Date = 08/30/14 Pct Recovery = 48% Analysis Date = 08/20/14 Pct Recovery = 48% Analysis Date = 08/20/14 Pct Recovery = 48% Analysis Date = 08/11/14 Pct Recovery = 48% Analysis Date = 08/11/14 Pct Recovery = 48% Analysis Date = 08/02/14 Pct Recovery = 48% Analysis Date = 08/02/14 Pct Recovery = 48% Analysis Date = 07/23/14 Pct Recovery = 48% Analysis Date = 07/23/14 Pct Recovery = 48% Analysis Date = 07/14/14 Pct Recovery = 48% Analysis Date = 07/14/14 Pct Recovery = 48% Analysis Date = 07/04/14 Pct Recovery = 48% Analysis Date = 07/04/14 Pct Recovery = 48% Analysis Date = 06/25/14 Pct Recovery = 48% Analysis Date = 06/25/14 Pct Recovery = 48% Analysis Date = 06/16/14 Pct Recovery = 48% Analysis Date = 06/16/14 Pct Recovery = 48% Analysis Date = 06/06/14 Pct Recovery = 48% Analysis Date = 06/06/14 Pct Recovery = 48% Analysis Date = 05/28/14 Pct Recovery = 49% Analysis Date = 05/28/14 Pct Recovery = 49% Analysis Date = 05/18/14 Pct Recovery = 49% Analysis Date = 05/18/14 Pct Recovery = 49% Analysis Date = 05/09/14 Pct Recovery = 49% Analysis Date = 05/09/14 Pct Recovery = 49% Analysis Date = 04/30/14 Pct Recovery = 49% Analysis Date = 04/30/14 Pct Recovery = 49% Analysis Date = 04/20/14 Pct Recovery = 49% Analysis Date = 04/20/14 Pct Recovery = 49% Analysis Date = 04/11/14 Pct Recovery = 50% Analysis Date = 04/11/14 Pct Recovery = 50% Analysis Date = 04/01/14 Pct Recovery = 50% Analysis Date = 04/01/14 Pct Recovery = 50% Analysis Date = 03/23/14 Pct Recovery = 50% Analysis Date = 03/23/14 Pct Recovery = 50% Analysis Date = 03/14/14 Pct Recovery = 51% Analysis Date = 03/14/14 Pct Recovery = 51% Analysis Date = 03/04/14 Pct Recovery = 51% Analysis Date = 03/04/14 Pct Recovery = 51% Analysis Date = 02/23/14 Pct Recovery = 52% Analysis Date = 02/23/14 Pct Recovery = 52% Analysis Date = 02/13/14 Pct Recovery = 52% Analysis Date = 02/13/14 Pct Recovery = 52% Analysis Date = 02/04/14 Pct Recovery = 52% Analysis Date = 02/04/14 Pct Recovery = 52% Analysis Date = 01/26/14 Pct Recovery = 53% Analysis Date = 01/26/14 Pct Recovery = 53% Analysis Date = 01/16/14 Pct Recovery = 53% Analysis Date = 01/16/14 Pct Recovery = 53% Analysis Date = 01/07/14 Pct Recovery = 53% Analysis Date = 01/07/14 Pct Recovery = 53% Analysis Date = 12/28/13 Pct Recovery = 54% Analysis Date = 12/28/13 Pct Recovery = 54% Analysis Date = 12/19/13 Pct Recovery = 54% Analysis Date = 12/19/13 Pct Recovery = 54% Analysis Date = 12/10/13 Pct Recovery = 54% Analysis Date = 12/10/13 Pct Recovery = 54% Analysis Date = 11/30/13 Pct Recovery = 55% Analysis Date = 11/30/13 Pct Recovery = 55% Analysis Date = 11/21/13 Pct Recovery = 55% Analysis Date = 11/21/13 Pct Recovery = 55% Analysis Date = 11/11/13 Pct Recovery = 55% Analysis Date = 11/11/13 Pct Recovery = 55% Analysis Date = 11/02/13 Pct Recovery = 55% Analysis Date = 11/02/13 Pct Recovery = 55% Analysis Date = 10/24/13 Pct Recovery = 56% Analysis Date = 10/24/13 Pct Recovery = 56% Analysis Date = 10/14/13 Pct Recovery = 56% Analysis Date = 10/14/13 Pct Recovery = 56% Analysis Date = 10/05/13 Pct Recovery = 56% Analysis Date = 10/05/13 Pct Recovery = 56% Analysis Date = 09/25/13 Pct Recovery = 57% Analysis Date = 09/25/13 Pct Recovery = 57% Analysis Date = 09/16/13 Pct Recovery = 57% Analysis Date = 09/16/13 Pct Recovery = 57% Analysis Date = 09/07/13 Pct Recovery = 57% Analysis Date = 09/07/13 Pct Recovery = 57% Analysis Date = 08/28/13 Pct Recovery = 57% Analysis Date = 08/28/13 Pct Recovery = 57% Analysis Date = 08/19/13 Pct Recovery = 58% Analysis Date = 08/19/13 Pct Recovery = 58% Analysis Date = 08/09/13 Pct Recovery = 58% Analysis Date = 08/09/13 Pct Recovery = 58% Analysis Date = 07/31/13 Pct Recovery = 58% Analysis Date = 07/31/13 Pct Recovery = 58% Analysis Date = 07/22/13 Pct Recovery = 59% Analysis Date = 07/22/13 Pct Recovery = 59% Analysis Date = 07/12/13 Pct Recovery = 59% Analysis Date = 07/12/13 Pct Recovery = 59% Analysis Date = 07/03/13 Pct Recovery = 59% Analysis Date = 07/03/13 Pct Recovery = 59% Analysis Date = 06/23/13 Pct Recovery = 60% Analysis Date = 06/23/13 Pct Recovery = 60% Analysis Date = 06/14/13 Pct Recovery = 60% Analysis Date = 06/14/13 Pct Recovery = 60% Analysis Date = 06/05/13 Pct Recovery = 60% Analysis Date = 06/05/13 Pct Recovery = 60% Analysis Date = 05/26/13 Pct Recovery = 60% Analysis Date = 05/26/13 Pct Recovery = 60% Analysis Date = 05/17/13 Pct Recovery = 61% Analysis Date = 05/17/13 Pct Recovery = 61% Analysis Date = 05/07/13 Pct Recovery = 61% Analysis Date = 05/07/13 Pct Recovery = 61% Analysis Date = 04/28/13 Pct Recovery = 61% Analysis Date = 04/28/13 Pct Recovery = 61% Analysis Date = 04/19/13 Pct Recovery = 62% Analysis Date = 04/19/13 Pct Recovery = 62% Analysis Date = 04/09/13 Pct Recovery = 62% Analysis Date = 04/09/13 Pct Recovery = 62% Analysis Date = 03/31/13 Pct Recovery = 62% Analysis Date = 03/31/13 Pct Recovery = 62% Analysis Date = 03/21/13 Pct Recovery = 63% Analysis Date = 03/21/13 Pct Recovery = 63% Analysis Date = 03/12/13 Pct Recovery = 63% Analysis Date = 03/12/13 Pct Recovery = 63% Analysis Date = 03/03/13 Pct Recovery = 63% Analysis Date = 03/03/13 Pct Recovery = 63% Analysis Date = 02/21/13 Pct Recovery = 63% Analysis Date = 02/21/13 Pct Recovery = 63% Analysis Date = 02/12/13 Pct Recovery = 64% Analysis Date = 02/12/13 Pct Recovery = 64% Analysis Date = 02/02/13 Pct Recovery = 64% Analysis Date = 02/02/13 Pct Recovery = 64% Analysis Date = 01/24/13 Pct Recovery = 64% Analysis Date = 01/24/13 Pct Recovery = 64% Analysis Date = 01/15/13 Pct Recovery = 65% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
DEETHYLATRAZINE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 78 53% 15% 52% 14%
Total 78 53% 15% 52% 14%

Sample Statistics
DEETHYLATRAZINE

Characteristic N % % Basis
Plotted 78 100% Spiked
Estimated Values 78 100% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 78 .  
False Negatives 0 0% 0 out of 78
Not Spiked 40 .  
False Positives 0 0% 0 out of 40

OBSP Determination:
DESULFINYLFIPRONIL
METHOD: 2033 , TESTIDCODE: 62170GCM29

Laboratory ID = 20172510330 Lab Value = 0.118 Expected Conc. = 0.08 Report level label = 0.012 Pct Recovery = 147% Analysis Date = 12/29/17 SpikeMix = ChemService 6537100: 100 µl & Abs 071817Pest: 100 µl SpecificMix = 071817Pest Laboratory ID = 20162860079 Lab Value = 0.080 Expected Conc. = 0.08 Report level label = 0.012 Pct Recovery = 100% Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl SpecificMix = 5054800 Laboratory ID = 20161880109 Lab Value = 0.108 Expected Conc. = 0.08 Report level label = 0.012 Pct Recovery = 135% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl SpecificMix = 5054800 Laboratory ID = 20130940097 Lab Value = 0.055 Expected Conc. = 0.075 Report level label = 0.012 Pct Recovery = 74% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = 0507-12-04.2 Laboratory ID = 20123560092 Lab Value = 0.062 Expected Conc. = 0.075 Report level label = 0.012 Pct Recovery = 83% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = 0507-12-04.2 Laboratory ID = 20152750006 Lab Value = 0.066 Expected Conc. = 0.072 Report level label = 0.012 Pct Recovery = 91% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl SpecificMix = 040615 Laboratory ID = 20152610011 Lab Value = 0.051 Expected Conc. = 0.072 Report level label = 0.012 Pct Recovery = 70% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl SpecificMix = 040615 Laboratory ID = 20171380001 Lab Value = 0.042 Expected Conc. = 0.064 Report level label = 0.012 Pct Recovery = 66% Analysis Date = 06/07/17 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 5054800 Laboratory ID = 20170960001 Lab Value = 0.065 Expected Conc. = 0.064 Report level label = 0.012 Pct Recovery = 102% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl SpecificMix = 5054800 Laboratory ID = 20161740258 Lab Value = 0.044 Expected Conc. = 0.064 Report level label = 0.012 Pct Recovery = 68% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 5054800 Laboratory ID = 20150430092 Lab Value = 0.031 Expected Conc. = 0.048 Report level label = 0.012 Pct Recovery = 65% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl SpecificMix = E1140407002 Laboratory ID = 20143240095 Lab Value = 0.048 Expected Conc. = 0.048 Report level label = 0.012 Pct Recovery = 100% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl SpecificMix = 032714 Laboratory ID = 20143110108 Lab Value = 0.031 Expected Conc. = 0.048 Report level label = 0.012 Pct Recovery = 64% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl SpecificMix = E1140407002 Laboratory ID = 20142720002 Lab Value = 0.032 Expected Conc. = 0.048 Report level label = 0.012 Pct Recovery = 66% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl SpecificMix = E1140407002 Laboratory ID = 20142270001 Lab Value = 0.034 Expected Conc. = 0.048 Report level label = 0.012 Pct Recovery = 70% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl SpecificMix = 032714 Laboratory ID = 20141770149 Lab Value = 0.030 Expected Conc. = 0.048 Report level label = 0.012 Pct Recovery = 63% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl SpecificMix = E1140407002 Laboratory ID = 20141220025 Lab Value = 0.053 Expected Conc. = 0.048 Report level label = 0.012 Pct Recovery = 110% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl SpecificMix = 032714 Laboratory ID = 20161260151 Lab Value = 0.023 Expected Conc. = 0.036 Report level label = 0.012 Pct Recovery = 65% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = EN150513008 Laboratory ID = 20160770090 Lab Value = 0.024 Expected Conc. = 0.036 Report level label = 0.012 Pct Recovery = 67% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = EN150513008 Laboratory ID = 20153510109 Lab Value = 0.021 Expected Conc. = 0.036 Report level label = 0.012 Pct Recovery = 58% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = EN150513008 Laboratory ID = 20152330039 Lab Value = 0.026 Expected Conc. = 0.036 Report level label = 0.012 Pct Recovery = 72% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl SpecificMix = EN150513008 Laboratory ID = 20151900132 Lab Value = 0.036 Expected Conc. = 0.036 Report level label = 0.012 Pct Recovery = 99% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl SpecificMix = 040615 Laboratory ID = 20151550293 Lab Value = 0.032 Expected Conc. = 0.036 Report level label = 0.012 Pct Recovery = 89% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl SpecificMix = 040615 Laboratory ID = 20171940002 Lab Value = 0.040 Expected Conc. = 0.032 Report level label = 0.012 Pct Recovery = 126% Analysis Date = 11/10/17 SpikeMix = ChemService 5054800: 40 µl & NSI 041816: 40 µl SpecificMix = 5054800 Laboratory ID = 20170460061 Lab Value = 0.030 Expected Conc. = 0.032 Report level label = 0.012 Pct Recovery = 93% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl SpecificMix = 5054800 Laboratory ID = 20163560019 Lab Value = 0.025 Expected Conc. = 0.032 Report level label = 0.012 Pct Recovery = 78% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl SpecificMix = 5054800 Laboratory ID = 20162150213 Lab Value = 0.024 Expected Conc. = 0.032 Report level label = 0.012 Pct Recovery = 75% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl SpecificMix = 5054800 Laboratory ID = 20130510051 Lab Value = 0.025 Expected Conc. = 0.03 Report level label = 0.012 Pct Recovery = 83% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl SpecificMix = 0507-12-04.2 Laboratory ID = 20172780018 Lab Value = 0.020 Expected Conc. = 0.024 Report level label = 0.012 Pct Recovery = 83% Analysis Date = 02/08/18 SpikeMix = ChemService 6537100: 30 µl & Abs 071817Pest: 30 µl SpecificMix = 071817Pest Laboratory ID = 20150150115 Lab Value = 0.017 Expected Conc. = 0.024 Report level label = 0.012 Pct Recovery = 72% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl SpecificMix = 032714 Laboratory ID = 20142820151 Lab Value = 0.020 Expected Conc. = 0.024 Report level label = 0.012 Pct Recovery = 84% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl SpecificMix = 032714 Laboratory ID = 20142470041 Lab Value = 0.019 Expected Conc. = 0.024 Report level label = 0.012 Pct Recovery = 79% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141910243 Lab Value = 0.014 Expected Conc. = 0.024 Report level label = 0.012 Pct Recovery = 57% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141640076 Lab Value = 0.016 Expected Conc. = 0.024 Report level label = 0.012 Pct Recovery = 67% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141490205 Lab Value = 0.022 Expected Conc. = 0.024 Report level label = 0.012 Pct Recovery = 92% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = 032714 Laboratory ID = 20141360094 Lab Value = 0.015 Expected Conc. = 0.024 Report level label = 0.012 Pct Recovery = 61% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141080004 Lab Value = 0.021 Expected Conc. = 0.024 Report level label = 0.012 Pct Recovery = 87% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl SpecificMix = 032714 Laboratory ID = 20161050143 Lab Value = 0.016 Expected Conc. = 0.018 Report level label = 0.012 Pct Recovery = 88% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Laboratory ID = 20160430111 Lab Value = 0.015 Expected Conc. = 0.018 Report level label = 0.012 Pct Recovery = 82% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Laboratory ID = 20160560044 Lab Value = 0.013 Expected Conc. = 0.018 Report level label = 0.012 Pct Recovery = 73% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl SpecificMix = EN150513008 Laboratory ID = 20160070059 Lab Value = 0.015 Expected Conc. = 0.018 Report level label = 0.012 Pct Recovery = 85% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = 040615 Laboratory ID = 20153160001 Lab Value = 0.014 Expected Conc. = 0.018 Report level label = 0.012 Pct Recovery = 76% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = EN150513008 Laboratory ID = 20153030068 Lab Value = 0.014 Expected Conc. = 0.018 Report level label = 0.012 Pct Recovery = 78% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150513008 Laboratory ID = 20152190003 Lab Value = 0.010 Expected Conc. = 0.018 Report level label = 0.012 Pct Recovery = 57% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150513008 Laboratory ID = 20151480170 Lab Value = 0.013 Expected Conc. = 0.018 Report level label = 0.012 Pct Recovery = 69% Analysis Date = 06/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150513008 Laboratory ID = 20151380009 Lab Value = 0.015 Expected Conc. = 0.018 Report level label = 0.012 Pct Recovery = 82% Analysis Date = 05/30/15 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Laboratory ID = 20151210037 Lab Value = 0.016 Expected Conc. = 0.018 Report level label = 0.012 Pct Recovery = 87% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Analysis Date = 02/08/18 Pct Recovery = 112% Analysis Date = 01/29/18 Pct Recovery = 112% Analysis Date = 01/29/18 Pct Recovery = 112% Analysis Date = 01/20/18 Pct Recovery = 111% Analysis Date = 01/20/18 Pct Recovery = 111% Analysis Date = 01/11/18 Pct Recovery = 111% Analysis Date = 01/11/18 Pct Recovery = 111% Analysis Date = 01/02/18 Pct Recovery = 110% Analysis Date = 01/02/18 Pct Recovery = 110% Analysis Date = 12/23/17 Pct Recovery = 110% Analysis Date = 12/23/17 Pct Recovery = 110% Analysis Date = 12/14/17 Pct Recovery = 109% Analysis Date = 12/14/17 Pct Recovery = 109% Analysis Date = 12/05/17 Pct Recovery = 109% Analysis Date = 12/05/17 Pct Recovery = 109% Analysis Date = 11/26/17 Pct Recovery = 108% Analysis Date = 11/26/17 Pct Recovery = 108% Analysis Date = 11/16/17 Pct Recovery = 108% Analysis Date = 11/16/17 Pct Recovery = 108% Analysis Date = 11/07/17 Pct Recovery = 107% Analysis Date = 11/07/17 Pct Recovery = 107% Analysis Date = 10/29/17 Pct Recovery = 107% Analysis Date = 10/29/17 Pct Recovery = 107% Analysis Date = 10/20/17 Pct Recovery = 106% Analysis Date = 10/20/17 Pct Recovery = 106% Analysis Date = 10/10/17 Pct Recovery = 106% Analysis Date = 10/10/17 Pct Recovery = 106% Analysis Date = 10/01/17 Pct Recovery = 105% Analysis Date = 10/01/17 Pct Recovery = 105% Analysis Date = 09/22/17 Pct Recovery = 105% Analysis Date = 09/22/17 Pct Recovery = 105% Analysis Date = 09/13/17 Pct Recovery = 104% Analysis Date = 09/13/17 Pct Recovery = 104% Analysis Date = 09/03/17 Pct Recovery = 104% Analysis Date = 09/03/17 Pct Recovery = 104% Analysis Date = 08/25/17 Pct Recovery = 103% Analysis Date = 08/25/17 Pct Recovery = 103% Analysis Date = 08/16/17 Pct Recovery = 103% Analysis Date = 08/16/17 Pct Recovery = 103% Analysis Date = 08/07/17 Pct Recovery = 102% Analysis Date = 08/07/17 Pct Recovery = 102% Analysis Date = 07/28/17 Pct Recovery = 102% Analysis Date = 07/28/17 Pct Recovery = 102% Analysis Date = 07/19/17 Pct Recovery = 102% Analysis Date = 07/19/17 Pct Recovery = 102% Analysis Date = 07/10/17 Pct Recovery = 101% Analysis Date = 07/10/17 Pct Recovery = 101% Analysis Date = 07/01/17 Pct Recovery = 101% Analysis Date = 07/01/17 Pct Recovery = 101% Analysis Date = 06/21/17 Pct Recovery = 100% Analysis Date = 06/21/17 Pct Recovery = 100% Analysis Date = 06/12/17 Pct Recovery = 100% Analysis Date = 06/12/17 Pct Recovery = 100% Analysis Date = 06/03/17 Pct Recovery = 99% Analysis Date = 06/03/17 Pct Recovery = 99% Analysis Date = 05/25/17 Pct Recovery = 99% Analysis Date = 05/25/17 Pct Recovery = 99% Analysis Date = 05/15/17 Pct Recovery = 98% Analysis Date = 05/15/17 Pct Recovery = 98% Analysis Date = 05/06/17 Pct Recovery = 98% Analysis Date = 05/06/17 Pct Recovery = 98% Analysis Date = 04/27/17 Pct Recovery = 97% Analysis Date = 04/27/17 Pct Recovery = 97% Analysis Date = 04/18/17 Pct Recovery = 97% Analysis Date = 04/18/17 Pct Recovery = 97% Analysis Date = 04/08/17 Pct Recovery = 96% Analysis Date = 04/08/17 Pct Recovery = 96% Analysis Date = 03/30/17 Pct Recovery = 96% Analysis Date = 03/30/17 Pct Recovery = 96% Analysis Date = 03/21/17 Pct Recovery = 95% Analysis Date = 03/21/17 Pct Recovery = 95% Analysis Date = 03/12/17 Pct Recovery = 94% Analysis Date = 03/12/17 Pct Recovery = 94% Analysis Date = 03/02/17 Pct Recovery = 94% Analysis Date = 03/02/17 Pct Recovery = 94% Analysis Date = 02/21/17 Pct Recovery = 93% Analysis Date = 02/21/17 Pct Recovery = 93% Analysis Date = 02/12/17 Pct Recovery = 93% Analysis Date = 02/12/17 Pct Recovery = 93% Analysis Date = 02/03/17 Pct Recovery = 92% Analysis Date = 02/03/17 Pct Recovery = 92% Analysis Date = 01/24/17 Pct Recovery = 92% Analysis Date = 01/24/17 Pct Recovery = 92% Analysis Date = 01/15/17 Pct Recovery = 91% Analysis Date = 01/15/17 Pct Recovery = 91% Analysis Date = 01/06/17 Pct Recovery = 91% Analysis Date = 01/06/17 Pct Recovery = 91% Analysis Date = 12/28/16 Pct Recovery = 90% Analysis Date = 12/28/16 Pct Recovery = 90% Analysis Date = 12/18/16 Pct Recovery = 90% Analysis Date = 12/18/16 Pct Recovery = 90% Analysis Date = 12/09/16 Pct Recovery = 89% Analysis Date = 12/09/16 Pct Recovery = 89% Analysis Date = 11/30/16 Pct Recovery = 88% Analysis Date = 11/30/16 Pct Recovery = 88% Analysis Date = 11/21/16 Pct Recovery = 88% Analysis Date = 11/21/16 Pct Recovery = 88% Analysis Date = 11/11/16 Pct Recovery = 87% Analysis Date = 11/11/16 Pct Recovery = 87% Analysis Date = 11/02/16 Pct Recovery = 87% Analysis Date = 11/02/16 Pct Recovery = 87% Analysis Date = 10/24/16 Pct Recovery = 86% Analysis Date = 10/24/16 Pct Recovery = 86% Analysis Date = 10/15/16 Pct Recovery = 86% Analysis Date = 10/15/16 Pct Recovery = 86% Analysis Date = 10/05/16 Pct Recovery = 85% Analysis Date = 10/05/16 Pct Recovery = 85% Analysis Date = 09/26/16 Pct Recovery = 85% Analysis Date = 09/26/16 Pct Recovery = 85% Analysis Date = 09/17/16 Pct Recovery = 84% Analysis Date = 09/17/16 Pct Recovery = 84% Analysis Date = 09/08/16 Pct Recovery = 84% Analysis Date = 09/08/16 Pct Recovery = 84% Analysis Date = 08/29/16 Pct Recovery = 84% Analysis Date = 08/29/16 Pct Recovery = 84% Analysis Date = 08/20/16 Pct Recovery = 84% Analysis Date = 08/20/16 Pct Recovery = 84% Analysis Date = 08/11/16 Pct Recovery = 83% Analysis Date = 08/11/16 Pct Recovery = 83% Analysis Date = 08/02/16 Pct Recovery = 83% Analysis Date = 08/02/16 Pct Recovery = 83% Analysis Date = 07/23/16 Pct Recovery = 83% Analysis Date = 07/23/16 Pct Recovery = 83% Analysis Date = 07/14/16 Pct Recovery = 83% Analysis Date = 07/14/16 Pct Recovery = 83% Analysis Date = 07/05/16 Pct Recovery = 82% Analysis Date = 07/05/16 Pct Recovery = 82% Analysis Date = 06/26/16 Pct Recovery = 82% Analysis Date = 06/26/16 Pct Recovery = 82% Analysis Date = 06/16/16 Pct Recovery = 82% Analysis Date = 06/16/16 Pct Recovery = 82% Analysis Date = 06/07/16 Pct Recovery = 82% Analysis Date = 06/07/16 Pct Recovery = 82% Analysis Date = 05/29/16 Pct Recovery = 81% Analysis Date = 05/29/16 Pct Recovery = 81% Analysis Date = 05/20/16 Pct Recovery = 81% Analysis Date = 05/20/16 Pct Recovery = 81% Analysis Date = 05/10/16 Pct Recovery = 81% Analysis Date = 05/10/16 Pct Recovery = 81% Analysis Date = 05/01/16 Pct Recovery = 81% Analysis Date = 05/01/16 Pct Recovery = 81% Analysis Date = 04/22/16 Pct Recovery = 80% Analysis Date = 04/22/16 Pct Recovery = 80% Analysis Date = 04/13/16 Pct Recovery = 80% Analysis Date = 04/13/16 Pct Recovery = 80% Analysis Date = 04/03/16 Pct Recovery = 80% Analysis Date = 04/03/16 Pct Recovery = 80% Analysis Date = 03/25/16 Pct Recovery = 80% Analysis Date = 03/25/16 Pct Recovery = 80% Analysis Date = 03/16/16 Pct Recovery = 79% Analysis Date = 03/16/16 Pct Recovery = 79% Analysis Date = 03/07/16 Pct Recovery = 79% Analysis Date = 03/07/16 Pct Recovery = 79% Analysis Date = 02/26/16 Pct Recovery = 79% Analysis Date = 02/26/16 Pct Recovery = 79% Analysis Date = 02/17/16 Pct Recovery = 79% Analysis Date = 02/17/16 Pct Recovery = 79% Analysis Date = 02/08/16 Pct Recovery = 79% Analysis Date = 02/08/16 Pct Recovery = 79% Analysis Date = 01/30/16 Pct Recovery = 78% Analysis Date = 01/30/16 Pct Recovery = 78% Analysis Date = 01/20/16 Pct Recovery = 78% Analysis Date = 01/20/16 Pct Recovery = 78% Analysis Date = 01/11/16 Pct Recovery = 78% Analysis Date = 01/11/16 Pct Recovery = 78% Analysis Date = 01/02/16 Pct Recovery = 78% Analysis Date = 01/02/16 Pct Recovery = 78% Analysis Date = 12/24/15 Pct Recovery = 78% Analysis Date = 12/24/15 Pct Recovery = 78% Analysis Date = 12/14/15 Pct Recovery = 78% Analysis Date = 12/14/15 Pct Recovery = 78% Analysis Date = 12/05/15 Pct Recovery = 78% Analysis Date = 12/05/15 Pct Recovery = 78% Analysis Date = 11/26/15 Pct Recovery = 78% Analysis Date = 11/26/15 Pct Recovery = 78% Analysis Date = 11/17/15 Pct Recovery = 78% Analysis Date = 11/17/15 Pct Recovery = 78% Analysis Date = 11/07/15 Pct Recovery = 78% Analysis Date = 11/07/15 Pct Recovery = 78% Analysis Date = 10/29/15 Pct Recovery = 78% Analysis Date = 10/29/15 Pct Recovery = 78% Analysis Date = 10/20/15 Pct Recovery = 78% Analysis Date = 10/20/15 Pct Recovery = 78% Analysis Date = 10/11/15 Pct Recovery = 78% Analysis Date = 10/11/15 Pct Recovery = 78% Analysis Date = 10/01/15 Pct Recovery = 77% Analysis Date = 10/01/15 Pct Recovery = 77% Analysis Date = 09/22/15 Pct Recovery = 77% Analysis Date = 09/22/15 Pct Recovery = 77% Analysis Date = 09/13/15 Pct Recovery = 77% Analysis Date = 09/13/15 Pct Recovery = 77% Analysis Date = 09/04/15 Pct Recovery = 77% Analysis Date = 09/04/15 Pct Recovery = 77% Analysis Date = 08/25/15 Pct Recovery = 77% Analysis Date = 08/25/15 Pct Recovery = 77% Analysis Date = 08/16/15 Pct Recovery = 77% Analysis Date = 08/16/15 Pct Recovery = 77% Analysis Date = 08/07/15 Pct Recovery = 77% Analysis Date = 08/07/15 Pct Recovery = 77% Analysis Date = 07/29/15 Pct Recovery = 77% Analysis Date = 07/29/15 Pct Recovery = 77% Analysis Date = 07/19/15 Pct Recovery = 77% Analysis Date = 07/19/15 Pct Recovery = 77% Analysis Date = 07/10/15 Pct Recovery = 77% Analysis Date = 07/10/15 Pct Recovery = 77% Analysis Date = 07/01/15 Pct Recovery = 77% Analysis Date = 07/01/15 Pct Recovery = 77% Analysis Date = 06/22/15 Pct Recovery = 77% Analysis Date = 06/22/15 Pct Recovery = 77% Analysis Date = 06/12/15 Pct Recovery = 77% Analysis Date = 06/12/15 Pct Recovery = 77% Analysis Date = 06/03/15 Pct Recovery = 77% Analysis Date = 06/03/15 Pct Recovery = 77% Analysis Date = 05/25/15 Pct Recovery = 77% Analysis Date = 05/25/15 Pct Recovery = 77% Analysis Date = 05/16/15 Pct Recovery = 77% Analysis Date = 05/16/15 Pct Recovery = 77% Analysis Date = 05/06/15 Pct Recovery = 77% Analysis Date = 05/06/15 Pct Recovery = 77% Analysis Date = 04/27/15 Pct Recovery = 77% Analysis Date = 04/27/15 Pct Recovery = 77% Analysis Date = 04/18/15 Pct Recovery = 77% Analysis Date = 04/18/15 Pct Recovery = 77% Analysis Date = 04/09/15 Pct Recovery = 77% Analysis Date = 04/09/15 Pct Recovery = 77% Analysis Date = 03/30/15 Pct Recovery = 77% Analysis Date = 03/30/15 Pct Recovery = 77% Analysis Date = 03/21/15 Pct Recovery = 77% Analysis Date = 03/21/15 Pct Recovery = 77% Analysis Date = 03/12/15 Pct Recovery = 77% Analysis Date = 03/12/15 Pct Recovery = 77% Analysis Date = 03/03/15 Pct Recovery = 77% Analysis Date = 03/03/15 Pct Recovery = 77% Analysis Date = 02/21/15 Pct Recovery = 77% Analysis Date = 02/21/15 Pct Recovery = 77% Analysis Date = 02/12/15 Pct Recovery = 77% Analysis Date = 02/12/15 Pct Recovery = 77% Analysis Date = 02/03/15 Pct Recovery = 77% Analysis Date = 02/03/15 Pct Recovery = 77% Analysis Date = 01/25/15 Pct Recovery = 77% Analysis Date = 01/25/15 Pct Recovery = 77% Analysis Date = 01/15/15 Pct Recovery = 77% Analysis Date = 01/15/15 Pct Recovery = 77% Analysis Date = 01/06/15 Pct Recovery = 77% Analysis Date = 01/06/15 Pct Recovery = 77% Analysis Date = 12/28/14 Pct Recovery = 77% Analysis Date = 12/28/14 Pct Recovery = 77% Analysis Date = 12/19/14 Pct Recovery = 77% Analysis Date = 12/19/14 Pct Recovery = 77% Analysis Date = 12/09/14 Pct Recovery = 77% Analysis Date = 12/09/14 Pct Recovery = 77% Analysis Date = 11/30/14 Pct Recovery = 77% Analysis Date = 11/30/14 Pct Recovery = 77% Analysis Date = 11/21/14 Pct Recovery = 77% Analysis Date = 11/21/14 Pct Recovery = 77% Analysis Date = 11/12/14 Pct Recovery = 77% Analysis Date = 11/12/14 Pct Recovery = 77% Analysis Date = 11/02/14 Pct Recovery = 77% Analysis Date = 11/02/14 Pct Recovery = 77% Analysis Date = 10/24/14 Pct Recovery = 77% Analysis Date = 10/24/14 Pct Recovery = 77% Analysis Date = 10/15/14 Pct Recovery = 77% Analysis Date = 10/15/14 Pct Recovery = 77% Analysis Date = 10/06/14 Pct Recovery = 77% Analysis Date = 10/06/14 Pct Recovery = 77% Analysis Date = 09/26/14 Pct Recovery = 77% Analysis Date = 09/26/14 Pct Recovery = 77% Analysis Date = 09/17/14 Pct Recovery = 77% Analysis Date = 09/17/14 Pct Recovery = 77% Analysis Date = 09/08/14 Pct Recovery = 77% Analysis Date = 09/08/14 Pct Recovery = 77% Analysis Date = 08/30/14 Pct Recovery = 77% Analysis Date = 08/30/14 Pct Recovery = 77% Analysis Date = 08/20/14 Pct Recovery = 77% Analysis Date = 08/20/14 Pct Recovery = 77% Analysis Date = 08/11/14 Pct Recovery = 77% Analysis Date = 08/11/14 Pct Recovery = 77% Analysis Date = 08/02/14 Pct Recovery = 77% Analysis Date = 08/02/14 Pct Recovery = 77% Analysis Date = 07/24/14 Pct Recovery = 77% Analysis Date = 07/24/14 Pct Recovery = 77% Analysis Date = 07/14/14 Pct Recovery = 77% Analysis Date = 07/14/14 Pct Recovery = 77% Analysis Date = 07/05/14 Pct Recovery = 77% Analysis Date = 07/05/14 Pct Recovery = 77% Analysis Date = 06/26/14 Pct Recovery = 77% Analysis Date = 06/26/14 Pct Recovery = 77% Analysis Date = 06/17/14 Pct Recovery = 77% Analysis Date = 06/17/14 Pct Recovery = 77% Analysis Date = 06/07/14 Pct Recovery = 77% Analysis Date = 06/07/14 Pct Recovery = 77% Analysis Date = 05/29/14 Pct Recovery = 77% Analysis Date = 05/29/14 Pct Recovery = 77% Analysis Date = 05/20/14 Pct Recovery = 77% Analysis Date = 05/20/14 Pct Recovery = 77% Analysis Date = 05/11/14 Pct Recovery = 77% Analysis Date = 05/11/14 Pct Recovery = 77% Analysis Date = 05/01/14 Pct Recovery = 77% Analysis Date = 05/01/14 Pct Recovery = 77% Analysis Date = 04/22/14 Pct Recovery = 77% Analysis Date = 04/22/14 Pct Recovery = 77% Analysis Date = 04/13/14 Pct Recovery = 77% Analysis Date = 04/13/14 Pct Recovery = 77% Analysis Date = 04/04/14 Pct Recovery = 77% Analysis Date = 04/04/14 Pct Recovery = 77% Analysis Date = 03/25/14 Pct Recovery = 77% Analysis Date = 03/25/14 Pct Recovery = 77% Analysis Date = 03/16/14 Pct Recovery = 77% Analysis Date = 03/16/14 Pct Recovery = 77% Analysis Date = 03/07/14 Pct Recovery = 77% Analysis Date = 03/07/14 Pct Recovery = 77% Analysis Date = 02/26/14 Pct Recovery = 78% Analysis Date = 02/26/14 Pct Recovery = 78% Analysis Date = 02/16/14 Pct Recovery = 78% Analysis Date = 02/16/14 Pct Recovery = 78% Analysis Date = 02/07/14 Pct Recovery = 78% Analysis Date = 02/07/14 Pct Recovery = 78% Analysis Date = 01/29/14 Pct Recovery = 78% Analysis Date = 01/29/14 Pct Recovery = 78% Analysis Date = 01/20/14 Pct Recovery = 78% Analysis Date = 01/20/14 Pct Recovery = 78% Analysis Date = 01/10/14 Pct Recovery = 78% Analysis Date = 01/10/14 Pct Recovery = 78% Analysis Date = 01/01/14 Pct Recovery = 78% Analysis Date = 01/01/14 Pct Recovery = 78% Analysis Date = 12/23/13 Pct Recovery = 78% Analysis Date = 12/23/13 Pct Recovery = 78% Analysis Date = 12/14/13 Pct Recovery = 78% Analysis Date = 12/14/13 Pct Recovery = 78% Analysis Date = 12/04/13 Pct Recovery = 78% Analysis Date = 12/04/13 Pct Recovery = 78% Analysis Date = 11/25/13 Pct Recovery = 78% Analysis Date = 11/25/13 Pct Recovery = 78% Analysis Date = 11/16/13 Pct Recovery = 78% Analysis Date = 11/16/13 Pct Recovery = 78% Analysis Date = 11/07/13 Pct Recovery = 78% Analysis Date = 11/07/13 Pct Recovery = 78% Analysis Date = 10/28/13 Pct Recovery = 78% Analysis Date = 10/28/13 Pct Recovery = 78% Analysis Date = 10/19/13 Pct Recovery = 79% Analysis Date = 10/19/13 Pct Recovery = 79% Analysis Date = 10/10/13 Pct Recovery = 79% Analysis Date = 10/10/13 Pct Recovery = 79% Analysis Date = 10/01/13 Pct Recovery = 79% Analysis Date = 10/01/13 Pct Recovery = 79% Analysis Date = 09/21/13 Pct Recovery = 79% Analysis Date = 09/21/13 Pct Recovery = 79% Analysis Date = 09/12/13 Pct Recovery = 79% Analysis Date = 09/12/13 Pct Recovery = 79% Analysis Date = 09/03/13 Pct Recovery = 79% Analysis Date = 09/03/13 Pct Recovery = 79% Analysis Date = 08/25/13 Pct Recovery = 79% Analysis Date = 08/25/13 Pct Recovery = 79% Analysis Date = 08/15/13 Pct Recovery = 79% Analysis Date = 08/15/13 Pct Recovery = 79% Analysis Date = 08/06/13 Pct Recovery = 79% Analysis Date = 08/06/13 Pct Recovery = 79% Analysis Date = 07/28/13 Pct Recovery = 79% Analysis Date = 07/28/13 Pct Recovery = 79% Analysis Date = 07/19/13 Pct Recovery = 79% Analysis Date = 07/19/13 Pct Recovery = 79% Analysis Date = 07/09/13 Pct Recovery = 79% Analysis Date = 07/09/13 Pct Recovery = 79% Analysis Date = 06/30/13 Pct Recovery = 79% Analysis Date = 06/30/13 Pct Recovery = 79% Analysis Date = 06/21/13 Pct Recovery = 79% Analysis Date = 06/21/13 Pct Recovery = 79% Analysis Date = 06/12/13 Pct Recovery = 79% Analysis Date = 06/12/13 Pct Recovery = 79% Analysis Date = 06/02/13 Pct Recovery = 80% Analysis Date = 06/02/13 Pct Recovery = 80% Analysis Date = 05/24/13 Pct Recovery = 80% Analysis Date = 05/24/13 Pct Recovery = 80% Analysis Date = 05/15/13 Pct Recovery = 80% Analysis Date = 05/15/13 Pct Recovery = 80% Analysis Date = 05/06/13 Pct Recovery = 80% Analysis Date = 05/06/13 Pct Recovery = 80% Analysis Date = 04/26/13 Pct Recovery = 80% Analysis Date = 04/26/13 Pct Recovery = 80% Analysis Date = 04/17/13 Pct Recovery = 80% Analysis Date = 04/17/13 Pct Recovery = 80% Analysis Date = 04/08/13 Pct Recovery = 80% Analysis Date = 04/08/13 Pct Recovery = 80% Analysis Date = 03/30/13 Pct Recovery = 80% Analysis Date = 03/30/13 Pct Recovery = 80% Analysis Date = 03/20/13 Pct Recovery = 80% Analysis Date = 03/20/13 Pct Recovery = 80% Analysis Date = 03/11/13 Pct Recovery = 80% Analysis Date = 03/11/13 Pct Recovery = 80% Analysis Date = 03/02/13 Pct Recovery = 80% Analysis Date = 03/02/13 Pct Recovery = 80% Analysis Date = 02/21/13 Pct Recovery = 80% Analysis Date = 02/21/13 Pct Recovery = 80% Analysis Date = 02/11/13 Pct Recovery = 80% Analysis Date = 02/11/13 Pct Recovery = 80% Analysis Date = 02/02/13 Pct Recovery = 80% Analysis Date = 02/02/13 Pct Recovery = 80% Analysis Date = 01/24/13 Pct Recovery = 80% Analysis Date = 01/24/13 Pct Recovery = 80% Analysis Date = 01/15/13 Pct Recovery = 81% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
DESULFINYLFIPRONIL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 47 82% 19% 78% 16%
Total 47 82% 19% 78% 16%

Sample Statistics
DESULFINYLFIPRONIL

Characteristic N % % Basis
Plotted 47 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 47 .  
False Negatives 0 0% 0 out of 47
Not Spiked 71 .  
False Positives 1 1% 1 out of 71

OBSP Determination:
DESULFINYLFIPRONIL AMIDE
METHOD: 2033 , TESTIDCODE: 62169GCM29

Laboratory ID = 20152750006 Lab Value = 0.003 Expected Conc. = 0.1744 Report level label = 0.029 Pct Recovery = 2% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl SpecificMix = EN150514012 Laboratory ID = 20160070059 Lab Value = 0.005 Expected Conc. = 0.0436 Report level label = 0.029 Pct Recovery = 11% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = EN150514012 Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
DESULFINYLFIPRONIL AMIDE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 2 6% 6% 6% 7%
Total 2 6% 6% 6% 7%

Sample Statistics
DESULFINYLFIPRONIL AMIDE

Characteristic N % % Basis
Plotted 2 20% Spiked
Estimated Values 2 20% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 10 .  
False Negatives 8 80% 8 out of 10
Not Spiked 108 .  
False Positives 0 0% 0 out of 108

OBSP Determination:
DIAZINON
METHOD: 2033 , TESTIDCODE: 39572GCM35

Laboratory ID = 20130250061 Lab Value = 0.132 Expected Conc. = 0.15 Report level label = 0.006 Pct Recovery = 88% Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl SpecificMix = A088380 Laboratory ID = 20140230082 Lab Value = 0.069 Expected Conc. = 0.075 Report level label = 0.006 Pct Recovery = 92% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl SpecificMix = A093651 Laboratory ID = 20132420001 Lab Value = 0.069 Expected Conc. = 0.075 Report level label = 0.006 Pct Recovery = 92% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl SpecificMix = A093651 Laboratory ID = 20130810108 Lab Value = 0.075 Expected Conc. = 0.075 Report level label = 0.006 Pct Recovery = 99% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl SpecificMix = T1120530013 Laboratory ID = 20123560092 Lab Value = 0.069 Expected Conc. = 0.075 Report level label = 0.006 Pct Recovery = 92% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = T1120530013 Laboratory ID = 20140100085 Lab Value = 0.069 Expected Conc. = 0.07 Report level label = 0.006 Pct Recovery = 99% Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl SpecificMix = T1130514013 Laboratory ID = 20132490342 Lab Value = 0.072 Expected Conc. = 0.07 Report level label = 0.006 Pct Recovery = 103% Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl SpecificMix = T1130514013 Laboratory ID = 20161880109 Lab Value = 0.045 Expected Conc. = 0.038 Report level label = 0.006 Pct Recovery = 119% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl SpecificMix = 03FF076 Laboratory ID = 20163370001 Lab Value = 0.036 Expected Conc. = 0.0375 Report level label = 0.006 Pct Recovery = 97% Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl SpecificMix = B20160331 Laboratory ID = 20163150006 Lab Value = 0.036 Expected Conc. = 0.0375 Report level label = 0.006 Pct Recovery = 95% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl SpecificMix = B20160331 Laboratory ID = 20131370001 Lab Value = 0.041 Expected Conc. = 0.0375 Report level label = 0.006 Pct Recovery = 109% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl SpecificMix = 1473000 Laboratory ID = 20152750006 Lab Value = 0.026 Expected Conc. = 0.036 Report level label = 0.006 Pct Recovery = 72% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl SpecificMix = 040615 Laboratory ID = 20152610011 Lab Value = 0.027 Expected Conc. = 0.036 Report level label = 0.006 Pct Recovery = 76% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl SpecificMix = 040615 Laboratory ID = 20140370077 Lab Value = 0.032 Expected Conc. = 0.035 Report level label = 0.006 Pct Recovery = 91% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl SpecificMix = T1130514013 Laboratory ID = 20132690010 Lab Value = 0.042 Expected Conc. = 0.035 Report level label = 0.006 Pct Recovery = 121% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl SpecificMix = T1130514013 Laboratory ID = 20170960001 Lab Value = 0.029 Expected Conc. = 0.0304 Report level label = 0.006 Pct Recovery = 95% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl SpecificMix = 03FF076 Laboratory ID = 20171720140 Lab Value = 0.033 Expected Conc. = 0.03 Report level label = 0.006 Pct Recovery = 109% Analysis Date = 08/31/17 SpikeMix = Supelco LC20138V: 80 µl & Phenova B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20171660002 Lab Value = 0.031 Expected Conc. = 0.03 Report level label = 0.006 Pct Recovery = 102% Analysis Date = 08/23/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20170190026 Lab Value = 0.029 Expected Conc. = 0.03 Report level label = 0.006 Pct Recovery = 97% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20161470001 Lab Value = 0.030 Expected Conc. = 0.03 Report level label = 0.006 Pct Recovery = 99% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20140860102 Lab Value = 0.026 Expected Conc. = 0.03 Report level label = 0.006 Pct Recovery = 85% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl SpecificMix = A093651 Laboratory ID = 20133400002 Lab Value = 0.030 Expected Conc. = 0.03 Report level label = 0.006 Pct Recovery = 99% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = A093651 Laboratory ID = 20132910008 Lab Value = 0.026 Expected Conc. = 0.03 Report level label = 0.006 Pct Recovery = 88% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = A093651 Laboratory ID = 20131920149 Lab Value = 0.029 Expected Conc. = 0.03 Report level label = 0.006 Pct Recovery = 98% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl SpecificMix = A093651 Laboratory ID = 20131230084 Lab Value = 0.032 Expected Conc. = 0.03 Report level label = 0.006 Pct Recovery = 107% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl SpecificMix = A088380 Laboratory ID = 20130650005 Lab Value = 0.025 Expected Conc. = 0.03 Report level label = 0.006 Pct Recovery = 83% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl SpecificMix = A088380 Laboratory ID = 20130390105 Lab Value = 0.027 Expected Conc. = 0.03 Report level label = 0.006 Pct Recovery = 89% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl SpecificMix = T1120530013 Laboratory ID = 20150720069 Lab Value = 0.019 Expected Conc. = 0.024 Report level label = 0.006 Pct Recovery = 80% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 03DD006 Laboratory ID = 20143110108 Lab Value = 0.019 Expected Conc. = 0.024 Report level label = 0.006 Pct Recovery = 78% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 03DD006 Laboratory ID = 20142960086 Lab Value = 0.019 Expected Conc. = 0.024 Report level label = 0.006 Pct Recovery = 80% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 03DD006 Laboratory ID = 20142720002 Lab Value = 0.018 Expected Conc. = 0.024 Report level label = 0.006 Pct Recovery = 75% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl SpecificMix = LC06435 Laboratory ID = 20142530087 Lab Value = 0.018 Expected Conc. = 0.024 Report level label = 0.006 Pct Recovery = 77% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl SpecificMix = LC06435 Laboratory ID = 20142270001 Lab Value = 0.015 Expected Conc. = 0.024 Report level label = 0.006 Pct Recovery = 64% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl SpecificMix = 03DD006 Laboratory ID = 20141570088 Lab Value = 0.022 Expected Conc. = 0.024 Report level label = 0.006 Pct Recovery = 93% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl SpecificMix = LC06435 Laboratory ID = 20141220025 Lab Value = 0.022 Expected Conc. = 0.024 Report level label = 0.006 Pct Recovery = 93% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl SpecificMix = LC06435 Laboratory ID = 20172560101 Lab Value = 0.018 Expected Conc. = 0.0201 Report level label = 0.006 Pct Recovery = 90% Analysis Date = 12/22/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6567600: 50 µl SpecificMix = EN170808006 Laboratory ID = 20172370001 Lab Value = 0.020 Expected Conc. = 0.0201 Report level label = 0.006 Pct Recovery = 98% Analysis Date = 11/18/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6537100: 50 µl SpecificMix = EN170808006 Laboratory ID = 20172230001 Lab Value = 0.024 Expected Conc. = 0.02 Report level label = 0.006 Pct Recovery = 120% Analysis Date = 10/19/17 SpikeMix = ChemService 6472100: 50 µl & Abs 071717Pest: 50 µl SpecificMix = 6472100 Laboratory ID = 20161260151 Lab Value = 0.017 Expected Conc. = 0.018 Report level label = 0.006 Pct Recovery = 92% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = EN150513008 Laboratory ID = 20160770090 Lab Value = 0.017 Expected Conc. = 0.018 Report level label = 0.006 Pct Recovery = 93% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = EN150513008 Laboratory ID = 20153510109 Lab Value = 0.016 Expected Conc. = 0.018 Report level label = 0.006 Pct Recovery = 87% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = EN150513008 Laboratory ID = 20152330039 Lab Value = 0.013 Expected Conc. = 0.018 Report level label = 0.006 Pct Recovery = 74% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl SpecificMix = EN150513008 Laboratory ID = 20151900132 Lab Value = 0.015 Expected Conc. = 0.018 Report level label = 0.006 Pct Recovery = 81% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl SpecificMix = 040615 Laboratory ID = 20151550293 Lab Value = 0.018 Expected Conc. = 0.018 Report level label = 0.006 Pct Recovery = 99% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl SpecificMix = 040615 Laboratory ID = 20172020035 Lab Value = 0.019 Expected Conc. = 0.0152 Report level label = 0.006 Pct Recovery = 122% Analysis Date = 11/07/17 SpikeMix = Abs 071717Pest: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20171510080 Lab Value = 0.019 Expected Conc. = 0.0152 Report level label = 0.006 Pct Recovery = 122% Analysis Date = 06/09/17 SpikeMix = Supelco LC20138V: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20170460061 Lab Value = 0.016 Expected Conc. = 0.0152 Report level label = 0.006 Pct Recovery = 106% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl SpecificMix = 03FF076 Laboratory ID = 20162660005 Lab Value = 0.014 Expected Conc. = 0.0152 Report level label = 0.006 Pct Recovery = 95% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl SpecificMix = 03FF076 Laboratory ID = 20161600087 Lab Value = 0.017 Expected Conc. = 0.0152 Report level label = 0.006 Pct Recovery = 111% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20161340228 Lab Value = 0.015 Expected Conc. = 0.0152 Report level label = 0.006 Pct Recovery = 96% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl SpecificMix = 03FF076 Laboratory ID = 20161190075 Lab Value = 0.014 Expected Conc. = 0.0152 Report level label = 0.006 Pct Recovery = 89% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20171160110 Lab Value = 0.016 Expected Conc. = 0.015 Report level label = 0.006 Pct Recovery = 105% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = B20160331 Laboratory ID = 20162380004 Lab Value = 0.015 Expected Conc. = 0.015 Report level label = 0.006 Pct Recovery = 98% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = B20160331 Laboratory ID = 20162150213 Lab Value = 0.014 Expected Conc. = 0.015 Report level label = 0.006 Pct Recovery = 91% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl SpecificMix = B20160331 Laboratory ID = 20140730138 Lab Value = 0.015 Expected Conc. = 0.015 Report level label = 0.006 Pct Recovery = 102% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 1473000 Laboratory ID = 20133470008 Lab Value = 0.015 Expected Conc. = 0.015 Report level label = 0.006 Pct Recovery = 97% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl SpecificMix = 1473000 Laboratory ID = 20133310030 Lab Value = 0.016 Expected Conc. = 0.015 Report level label = 0.006 Pct Recovery = 104% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl SpecificMix = 1473000 Laboratory ID = 20131790009 Lab Value = 0.017 Expected Conc. = 0.015 Report level label = 0.006 Pct Recovery = 111% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl SpecificMix = 1473000 Laboratory ID = 20131650073 Lab Value = 0.017 Expected Conc. = 0.015 Report level label = 0.006 Pct Recovery = 115% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl SpecificMix = 1473000 Laboratory ID = 20133050050 Lab Value = 0.015 Expected Conc. = 0.014 Report level label = 0.006 Pct Recovery = 107% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl SpecificMix = T1130514013 Laboratory ID = 20132280016 Lab Value = 0.016 Expected Conc. = 0.014 Report level label = 0.006 Pct Recovery = 111% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl SpecificMix = T1130514013 Laboratory ID = 20173120093 Lab Value = 0.014 Expected Conc. = 0.012 Report level label = 0.006 Pct Recovery = 116% Analysis Date = 03/10/18 SpikeMix = ChemService 6472100: 30 µl & ChemService 6537100: 30 µl SpecificMix = 6472100 Laboratory ID = 20150150115 Lab Value = 0.010 Expected Conc. = 0.012 Report level label = 0.006 Pct Recovery = 82% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl SpecificMix = LC06435 Laboratory ID = 20143370094 Lab Value = 0.009 Expected Conc. = 0.012 Report level label = 0.006 Pct Recovery = 77% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl SpecificMix = LC06435 Laboratory ID = 20142200164 Lab Value = 0.011 Expected Conc. = 0.012 Report level label = 0.006 Pct Recovery = 92% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 03DD006 Laboratory ID = 20141910243 Lab Value = 0.009 Expected Conc. = 0.012 Report level label = 0.006 Pct Recovery = 73% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = LC06435 Laboratory ID = 20141840097 Lab Value = 0.010 Expected Conc. = 0.012 Report level label = 0.006 Pct Recovery = 83% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl SpecificMix = LC06435 Laboratory ID = 20141640076 Lab Value = 0.011 Expected Conc. = 0.012 Report level label = 0.006 Pct Recovery = 93% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = 03DD006 Laboratory ID = 20141420140 Lab Value = 0.012 Expected Conc. = 0.012 Report level label = 0.006 Pct Recovery = 100% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 03DD006 Laboratory ID = 20141080004 Lab Value = 0.010 Expected Conc. = 0.012 Report level label = 0.006 Pct Recovery = 87% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl SpecificMix = 03DD006 Laboratory ID = 20161050143 Lab Value = 0.010 Expected Conc. = 0.009 Report level label = 0.006 Pct Recovery = 109% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Laboratory ID = 20160430111 Lab Value = 0.009 Expected Conc. = 0.009 Report level label = 0.006 Pct Recovery = 100% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Laboratory ID = 20160560044 Lab Value = 0.008 Expected Conc. = 0.009 Report level label = 0.006 Pct Recovery = 91% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl SpecificMix = EN150513008 Laboratory ID = 20160070059 Lab Value = 0.009 Expected Conc. = 0.009 Report level label = 0.006 Pct Recovery = 104% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = 040615 Laboratory ID = 20153160001 Lab Value = 0.010 Expected Conc. = 0.009 Report level label = 0.006 Pct Recovery = 108% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = EN150513008 Laboratory ID = 20153030068 Lab Value = 0.010 Expected Conc. = 0.009 Report level label = 0.006 Pct Recovery = 106% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150513008 Laboratory ID = 20152190003 Lab Value = 0.007 Expected Conc. = 0.009 Report level label = 0.006 Pct Recovery = 78% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150513008 Laboratory ID = 20151480170 Lab Value = 0.008 Expected Conc. = 0.009 Report level label = 0.006 Pct Recovery = 93% Analysis Date = 06/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150513008 Laboratory ID = 20151380009 Lab Value = 0.008 Expected Conc. = 0.009 Report level label = 0.006 Pct Recovery = 88% Analysis Date = 05/30/15 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Laboratory ID = 20151210037 Lab Value = 0.009 Expected Conc. = 0.009 Report level label = 0.006 Pct Recovery = 103% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Analysis Date = 03/10/18 Pct Recovery = 111% Analysis Date = 02/28/18 Pct Recovery = 111% Analysis Date = 02/28/18 Pct Recovery = 111% Analysis Date = 02/19/18 Pct Recovery = 110% Analysis Date = 02/19/18 Pct Recovery = 110% Analysis Date = 02/09/18 Pct Recovery = 110% Analysis Date = 02/09/18 Pct Recovery = 110% Analysis Date = 01/31/18 Pct Recovery = 110% Analysis Date = 01/31/18 Pct Recovery = 110% Analysis Date = 01/22/18 Pct Recovery = 110% Analysis Date = 01/22/18 Pct Recovery = 110% Analysis Date = 01/12/18 Pct Recovery = 110% Analysis Date = 01/12/18 Pct Recovery = 110% Analysis Date = 01/03/18 Pct Recovery = 109% Analysis Date = 01/03/18 Pct Recovery = 109% Analysis Date = 12/24/17 Pct Recovery = 109% Analysis Date = 12/24/17 Pct Recovery = 109% Analysis Date = 12/15/17 Pct Recovery = 109% Analysis Date = 12/15/17 Pct Recovery = 109% Analysis Date = 12/06/17 Pct Recovery = 109% Analysis Date = 12/06/17 Pct Recovery = 109% Analysis Date = 11/26/17 Pct Recovery = 109% Analysis Date = 11/26/17 Pct Recovery = 109% Analysis Date = 11/17/17 Pct Recovery = 108% Analysis Date = 11/17/17 Pct Recovery = 108% Analysis Date = 11/07/17 Pct Recovery = 108% Analysis Date = 11/07/17 Pct Recovery = 108% Analysis Date = 10/29/17 Pct Recovery = 108% Analysis Date = 10/29/17 Pct Recovery = 108% Analysis Date = 10/20/17 Pct Recovery = 108% Analysis Date = 10/20/17 Pct Recovery = 108% Analysis Date = 10/10/17 Pct Recovery = 108% Analysis Date = 10/10/17 Pct Recovery = 108% Analysis Date = 10/01/17 Pct Recovery = 107% Analysis Date = 10/01/17 Pct Recovery = 107% Analysis Date = 09/21/17 Pct Recovery = 107% Analysis Date = 09/21/17 Pct Recovery = 107% Analysis Date = 09/12/17 Pct Recovery = 107% Analysis Date = 09/12/17 Pct Recovery = 107% Analysis Date = 09/03/17 Pct Recovery = 107% Analysis Date = 09/03/17 Pct Recovery = 107% Analysis Date = 08/24/17 Pct Recovery = 106% Analysis Date = 08/24/17 Pct Recovery = 106% Analysis Date = 08/15/17 Pct Recovery = 106% Analysis Date = 08/15/17 Pct Recovery = 106% Analysis Date = 08/05/17 Pct Recovery = 106% Analysis Date = 08/05/17 Pct Recovery = 106% Analysis Date = 07/27/17 Pct Recovery = 106% Analysis Date = 07/27/17 Pct Recovery = 106% Analysis Date = 07/18/17 Pct Recovery = 106% Analysis Date = 07/18/17 Pct Recovery = 106% Analysis Date = 07/08/17 Pct Recovery = 105% Analysis Date = 07/08/17 Pct Recovery = 105% Analysis Date = 06/29/17 Pct Recovery = 105% Analysis Date = 06/29/17 Pct Recovery = 105% Analysis Date = 06/19/17 Pct Recovery = 105% Analysis Date = 06/19/17 Pct Recovery = 105% Analysis Date = 06/10/17 Pct Recovery = 105% Analysis Date = 06/10/17 Pct Recovery = 105% Analysis Date = 06/01/17 Pct Recovery = 105% Analysis Date = 06/01/17 Pct Recovery = 105% Analysis Date = 05/22/17 Pct Recovery = 104% Analysis Date = 05/22/17 Pct Recovery = 104% Analysis Date = 05/13/17 Pct Recovery = 104% Analysis Date = 05/13/17 Pct Recovery = 104% Analysis Date = 05/03/17 Pct Recovery = 104% Analysis Date = 05/03/17 Pct Recovery = 104% Analysis Date = 04/24/17 Pct Recovery = 104% Analysis Date = 04/24/17 Pct Recovery = 104% Analysis Date = 04/15/17 Pct Recovery = 104% Analysis Date = 04/15/17 Pct Recovery = 104% Analysis Date = 04/05/17 Pct Recovery = 103% Analysis Date = 04/05/17 Pct Recovery = 103% Analysis Date = 03/27/17 Pct Recovery = 103% Analysis Date = 03/27/17 Pct Recovery = 103% Analysis Date = 03/17/17 Pct Recovery = 103% Analysis Date = 03/17/17 Pct Recovery = 103% Analysis Date = 03/08/17 Pct Recovery = 103% Analysis Date = 03/08/17 Pct Recovery = 103% Analysis Date = 02/27/17 Pct Recovery = 102% Analysis Date = 02/27/17 Pct Recovery = 102% Analysis Date = 02/17/17 Pct Recovery = 102% Analysis Date = 02/17/17 Pct Recovery = 102% Analysis Date = 02/08/17 Pct Recovery = 102% Analysis Date = 02/08/17 Pct Recovery = 102% Analysis Date = 01/29/17 Pct Recovery = 102% Analysis Date = 01/29/17 Pct Recovery = 102% Analysis Date = 01/20/17 Pct Recovery = 102% Analysis Date = 01/20/17 Pct Recovery = 102% Analysis Date = 01/11/17 Pct Recovery = 101% Analysis Date = 01/11/17 Pct Recovery = 101% Analysis Date = 01/01/17 Pct Recovery = 101% Analysis Date = 01/01/17 Pct Recovery = 101% Analysis Date = 12/23/16 Pct Recovery = 101% Analysis Date = 12/23/16 Pct Recovery = 101% Analysis Date = 12/13/16 Pct Recovery = 101% Analysis Date = 12/13/16 Pct Recovery = 101% Analysis Date = 12/04/16 Pct Recovery = 100% Analysis Date = 12/04/16 Pct Recovery = 100% Analysis Date = 11/25/16 Pct Recovery = 100% Analysis Date = 11/25/16 Pct Recovery = 100% Analysis Date = 11/15/16 Pct Recovery = 100% Analysis Date = 11/15/16 Pct Recovery = 100% Analysis Date = 11/06/16 Pct Recovery = 100% Analysis Date = 11/06/16 Pct Recovery = 100% Analysis Date = 10/27/16 Pct Recovery = 100% Analysis Date = 10/27/16 Pct Recovery = 100% Analysis Date = 10/18/16 Pct Recovery = 99% Analysis Date = 10/18/16 Pct Recovery = 99% Analysis Date = 10/09/16 Pct Recovery = 99% Analysis Date = 10/09/16 Pct Recovery = 99% Analysis Date = 09/29/16 Pct Recovery = 99% Analysis Date = 09/29/16 Pct Recovery = 99% Analysis Date = 09/20/16 Pct Recovery = 99% Analysis Date = 09/20/16 Pct Recovery = 99% Analysis Date = 09/10/16 Pct Recovery = 98% Analysis Date = 09/10/16 Pct Recovery = 98% Analysis Date = 09/01/16 Pct Recovery = 98% Analysis Date = 09/01/16 Pct Recovery = 98% Analysis Date = 08/23/16 Pct Recovery = 98% Analysis Date = 08/23/16 Pct Recovery = 98% Analysis Date = 08/13/16 Pct Recovery = 98% Analysis Date = 08/13/16 Pct Recovery = 98% Analysis Date = 08/04/16 Pct Recovery = 98% Analysis Date = 08/04/16 Pct Recovery = 98% Analysis Date = 07/25/16 Pct Recovery = 97% Analysis Date = 07/25/16 Pct Recovery = 97% Analysis Date = 07/16/16 Pct Recovery = 97% Analysis Date = 07/16/16 Pct Recovery = 97% Analysis Date = 07/07/16 Pct Recovery = 97% Analysis Date = 07/07/16 Pct Recovery = 97% Analysis Date = 06/27/16 Pct Recovery = 97% Analysis Date = 06/27/16 Pct Recovery = 97% Analysis Date = 06/18/16 Pct Recovery = 96% Analysis Date = 06/18/16 Pct Recovery = 96% Analysis Date = 06/08/16 Pct Recovery = 96% Analysis Date = 06/08/16 Pct Recovery = 96% Analysis Date = 05/30/16 Pct Recovery = 96% Analysis Date = 05/30/16 Pct Recovery = 96% Analysis Date = 05/21/16 Pct Recovery = 96% Analysis Date = 05/21/16 Pct Recovery = 96% Analysis Date = 05/11/16 Pct Recovery = 96% Analysis Date = 05/11/16 Pct Recovery = 96% Analysis Date = 05/02/16 Pct Recovery = 95% Analysis Date = 05/02/16 Pct Recovery = 95% Analysis Date = 04/22/16 Pct Recovery = 95% Analysis Date = 04/22/16 Pct Recovery = 95% Analysis Date = 04/13/16 Pct Recovery = 95% Analysis Date = 04/13/16 Pct Recovery = 95% Analysis Date = 04/04/16 Pct Recovery = 95% Analysis Date = 04/04/16 Pct Recovery = 95% Analysis Date = 03/25/16 Pct Recovery = 94% Analysis Date = 03/25/16 Pct Recovery = 94% Analysis Date = 03/16/16 Pct Recovery = 94% Analysis Date = 03/16/16 Pct Recovery = 94% Analysis Date = 03/06/16 Pct Recovery = 94% Analysis Date = 03/06/16 Pct Recovery = 94% Analysis Date = 02/26/16 Pct Recovery = 94% Analysis Date = 02/26/16 Pct Recovery = 94% Analysis Date = 02/17/16 Pct Recovery = 93% Analysis Date = 02/17/16 Pct Recovery = 93% Analysis Date = 02/07/16 Pct Recovery = 93% Analysis Date = 02/07/16 Pct Recovery = 93% Analysis Date = 01/29/16 Pct Recovery = 93% Analysis Date = 01/29/16 Pct Recovery = 93% Analysis Date = 01/19/16 Pct Recovery = 93% Analysis Date = 01/19/16 Pct Recovery = 93% Analysis Date = 01/10/16 Pct Recovery = 93% Analysis Date = 01/10/16 Pct Recovery = 93% Analysis Date = 01/01/16 Pct Recovery = 92% Analysis Date = 01/01/16 Pct Recovery = 92% Analysis Date = 12/22/15 Pct Recovery = 92% Analysis Date = 12/22/15 Pct Recovery = 92% Analysis Date = 12/13/15 Pct Recovery = 92% Analysis Date = 12/13/15 Pct Recovery = 92% Analysis Date = 12/03/15 Pct Recovery = 92% Analysis Date = 12/03/15 Pct Recovery = 92% Analysis Date = 11/24/15 Pct Recovery = 91% Analysis Date = 11/24/15 Pct Recovery = 91% Analysis Date = 11/15/15 Pct Recovery = 91% Analysis Date = 11/15/15 Pct Recovery = 91% Analysis Date = 11/05/15 Pct Recovery = 91% Analysis Date = 11/05/15 Pct Recovery = 91% Analysis Date = 10/27/15 Pct Recovery = 91% Analysis Date = 10/27/15 Pct Recovery = 91% Analysis Date = 10/17/15 Pct Recovery = 90% Analysis Date = 10/17/15 Pct Recovery = 90% Analysis Date = 10/08/15 Pct Recovery = 90% Analysis Date = 10/08/15 Pct Recovery = 90% Analysis Date = 09/29/15 Pct Recovery = 90% Analysis Date = 09/29/15 Pct Recovery = 90% Analysis Date = 09/19/15 Pct Recovery = 90% Analysis Date = 09/19/15 Pct Recovery = 90% Analysis Date = 09/10/15 Pct Recovery = 89% Analysis Date = 09/10/15 Pct Recovery = 89% Analysis Date = 08/31/15 Pct Recovery = 89% Analysis Date = 08/31/15 Pct Recovery = 89% Analysis Date = 08/22/15 Pct Recovery = 89% Analysis Date = 08/22/15 Pct Recovery = 89% Analysis Date = 08/13/15 Pct Recovery = 89% Analysis Date = 08/13/15 Pct Recovery = 89% Analysis Date = 08/03/15 Pct Recovery = 89% Analysis Date = 08/03/15 Pct Recovery = 89% Analysis Date = 07/25/15 Pct Recovery = 88% Analysis Date = 07/25/15 Pct Recovery = 88% Analysis Date = 07/15/15 Pct Recovery = 88% Analysis Date = 07/15/15 Pct Recovery = 88% Analysis Date = 07/06/15 Pct Recovery = 88% Analysis Date = 07/06/15 Pct Recovery = 88% Analysis Date = 06/27/15 Pct Recovery = 88% Analysis Date = 06/27/15 Pct Recovery = 88% Analysis Date = 06/17/15 Pct Recovery = 88% Analysis Date = 06/17/15 Pct Recovery = 88% Analysis Date = 06/08/15 Pct Recovery = 87% Analysis Date = 06/08/15 Pct Recovery = 87% Analysis Date = 05/29/15 Pct Recovery = 87% Analysis Date = 05/29/15 Pct Recovery = 87% Analysis Date = 05/20/15 Pct Recovery = 87% Analysis Date = 05/20/15 Pct Recovery = 87% Analysis Date = 05/11/15 Pct Recovery = 87% Analysis Date = 05/11/15 Pct Recovery = 87% Analysis Date = 05/01/15 Pct Recovery = 87% Analysis Date = 05/01/15 Pct Recovery = 87% Analysis Date = 04/22/15 Pct Recovery = 86% Analysis Date = 04/22/15 Pct Recovery = 86% Analysis Date = 04/12/15 Pct Recovery = 86% Analysis Date = 04/12/15 Pct Recovery = 86% Analysis Date = 04/03/15 Pct Recovery = 86% Analysis Date = 04/03/15 Pct Recovery = 86% Analysis Date = 03/25/15 Pct Recovery = 86% Analysis Date = 03/25/15 Pct Recovery = 86% Analysis Date = 03/15/15 Pct Recovery = 86% Analysis Date = 03/15/15 Pct Recovery = 86% Analysis Date = 03/06/15 Pct Recovery = 86% Analysis Date = 03/06/15 Pct Recovery = 86% Analysis Date = 02/24/15 Pct Recovery = 86% Analysis Date = 02/24/15 Pct Recovery = 86% Analysis Date = 02/15/15 Pct Recovery = 86% Analysis Date = 02/15/15 Pct Recovery = 86% Analysis Date = 02/06/15 Pct Recovery = 86% Analysis Date = 02/06/15 Pct Recovery = 86% Analysis Date = 01/27/15 Pct Recovery = 86% Analysis Date = 01/27/15 Pct Recovery = 86% Analysis Date = 01/18/15 Pct Recovery = 86% Analysis Date = 01/18/15 Pct Recovery = 86% Analysis Date = 01/08/15 Pct Recovery = 86% Analysis Date = 01/08/15 Pct Recovery = 86% Analysis Date = 12/30/14 Pct Recovery = 86% Analysis Date = 12/30/14 Pct Recovery = 86% Analysis Date = 12/21/14 Pct Recovery = 86% Analysis Date = 12/21/14 Pct Recovery = 86% Analysis Date = 12/11/14 Pct Recovery = 86% Analysis Date = 12/11/14 Pct Recovery = 86% Analysis Date = 12/02/14 Pct Recovery = 86% Analysis Date = 12/02/14 Pct Recovery = 86% Analysis Date = 11/22/14 Pct Recovery = 86% Analysis Date = 11/22/14 Pct Recovery = 86% Analysis Date = 11/13/14 Pct Recovery = 86% Analysis Date = 11/13/14 Pct Recovery = 86% Analysis Date = 11/04/14 Pct Recovery = 87% Analysis Date = 11/04/14 Pct Recovery = 87% Analysis Date = 10/25/14 Pct Recovery = 87% Analysis Date = 10/25/14 Pct Recovery = 87% Analysis Date = 10/16/14 Pct Recovery = 87% Analysis Date = 10/16/14 Pct Recovery = 87% Analysis Date = 10/06/14 Pct Recovery = 87% Analysis Date = 10/06/14 Pct Recovery = 87% Analysis Date = 09/27/14 Pct Recovery = 87% Analysis Date = 09/27/14 Pct Recovery = 87% Analysis Date = 09/18/14 Pct Recovery = 87% Analysis Date = 09/18/14 Pct Recovery = 87% Analysis Date = 09/08/14 Pct Recovery = 87% Analysis Date = 09/08/14 Pct Recovery = 87% Analysis Date = 08/30/14 Pct Recovery = 88% Analysis Date = 08/30/14 Pct Recovery = 88% Analysis Date = 08/20/14 Pct Recovery = 88% Analysis Date = 08/20/14 Pct Recovery = 88% Analysis Date = 08/11/14 Pct Recovery = 88% Analysis Date = 08/11/14 Pct Recovery = 88% Analysis Date = 08/02/14 Pct Recovery = 89% Analysis Date = 08/02/14 Pct Recovery = 89% Analysis Date = 07/23/14 Pct Recovery = 89% Analysis Date = 07/23/14 Pct Recovery = 89% Analysis Date = 07/14/14 Pct Recovery = 89% Analysis Date = 07/14/14 Pct Recovery = 89% Analysis Date = 07/04/14 Pct Recovery = 89% Analysis Date = 07/04/14 Pct Recovery = 89% Analysis Date = 06/25/14 Pct Recovery = 90% Analysis Date = 06/25/14 Pct Recovery = 90% Analysis Date = 06/16/14 Pct Recovery = 90% Analysis Date = 06/16/14 Pct Recovery = 90% Analysis Date = 06/06/14 Pct Recovery = 90% Analysis Date = 06/06/14 Pct Recovery = 90% Analysis Date = 05/28/14 Pct Recovery = 90% Analysis Date = 05/28/14 Pct Recovery = 90% Analysis Date = 05/18/14 Pct Recovery = 91% Analysis Date = 05/18/14 Pct Recovery = 91% Analysis Date = 05/09/14 Pct Recovery = 91% Analysis Date = 05/09/14 Pct Recovery = 91% Analysis Date = 04/30/14 Pct Recovery = 91% Analysis Date = 04/30/14 Pct Recovery = 91% Analysis Date = 04/20/14 Pct Recovery = 91% Analysis Date = 04/20/14 Pct Recovery = 91% Analysis Date = 04/11/14 Pct Recovery = 92% Analysis Date = 04/11/14 Pct Recovery = 92% Analysis Date = 04/01/14 Pct Recovery = 92% Analysis Date = 04/01/14 Pct Recovery = 92% Analysis Date = 03/23/14 Pct Recovery = 92% Analysis Date = 03/23/14 Pct Recovery = 92% Analysis Date = 03/14/14 Pct Recovery = 93% Analysis Date = 03/14/14 Pct Recovery = 93% Analysis Date = 03/04/14 Pct Recovery = 93% Analysis Date = 03/04/14 Pct Recovery = 93% Analysis Date = 02/23/14 Pct Recovery = 93% Analysis Date = 02/23/14 Pct Recovery = 93% Analysis Date = 02/13/14 Pct Recovery = 93% Analysis Date = 02/13/14 Pct Recovery = 93% Analysis Date = 02/04/14 Pct Recovery = 94% Analysis Date = 02/04/14 Pct Recovery = 94% Analysis Date = 01/26/14 Pct Recovery = 94% Analysis Date = 01/26/14 Pct Recovery = 94% Analysis Date = 01/16/14 Pct Recovery = 94% Analysis Date = 01/16/14 Pct Recovery = 94% Analysis Date = 01/07/14 Pct Recovery = 95% Analysis Date = 01/07/14 Pct Recovery = 95% Analysis Date = 12/28/13 Pct Recovery = 95% Analysis Date = 12/28/13 Pct Recovery = 95% Analysis Date = 12/19/13 Pct Recovery = 95% Analysis Date = 12/19/13 Pct Recovery = 95% Analysis Date = 12/10/13 Pct Recovery = 95% Analysis Date = 12/10/13 Pct Recovery = 95% Analysis Date = 11/30/13 Pct Recovery = 96% Analysis Date = 11/30/13 Pct Recovery = 96% Analysis Date = 11/21/13 Pct Recovery = 96% Analysis Date = 11/21/13 Pct Recovery = 96% Analysis Date = 11/11/13 Pct Recovery = 96% Analysis Date = 11/11/13 Pct Recovery = 96% Analysis Date = 11/02/13 Pct Recovery = 96% Analysis Date = 11/02/13 Pct Recovery = 96% Analysis Date = 10/24/13 Pct Recovery = 97% Analysis Date = 10/24/13 Pct Recovery = 97% Analysis Date = 10/14/13 Pct Recovery = 97% Analysis Date = 10/14/13 Pct Recovery = 97% Analysis Date = 10/05/13 Pct Recovery = 97% Analysis Date = 10/05/13 Pct Recovery = 97% Analysis Date = 09/25/13 Pct Recovery = 97% Analysis Date = 09/25/13 Pct Recovery = 97% Analysis Date = 09/16/13 Pct Recovery = 98% Analysis Date = 09/16/13 Pct Recovery = 98% Analysis Date = 09/07/13 Pct Recovery = 98% Analysis Date = 09/07/13 Pct Recovery = 98% Analysis Date = 08/28/13 Pct Recovery = 98% Analysis Date = 08/28/13 Pct Recovery = 98% Analysis Date = 08/19/13 Pct Recovery = 98% Analysis Date = 08/19/13 Pct Recovery = 98% Analysis Date = 08/09/13 Pct Recovery = 99% Analysis Date = 08/09/13 Pct Recovery = 99% Analysis Date = 07/31/13 Pct Recovery = 99% Analysis Date = 07/31/13 Pct Recovery = 99% Analysis Date = 07/22/13 Pct Recovery = 99% Analysis Date = 07/22/13 Pct Recovery = 99% Analysis Date = 07/12/13 Pct Recovery = 99% Analysis Date = 07/12/13 Pct Recovery = 99% Analysis Date = 07/03/13 Pct Recovery = 100% Analysis Date = 07/03/13 Pct Recovery = 100% Analysis Date = 06/23/13 Pct Recovery = 100% Analysis Date = 06/23/13 Pct Recovery = 100% Analysis Date = 06/14/13 Pct Recovery = 100% Analysis Date = 06/14/13 Pct Recovery = 100% Analysis Date = 06/05/13 Pct Recovery = 100% Analysis Date = 06/05/13 Pct Recovery = 100% Analysis Date = 05/26/13 Pct Recovery = 101% Analysis Date = 05/26/13 Pct Recovery = 101% Analysis Date = 05/17/13 Pct Recovery = 101% Analysis Date = 05/17/13 Pct Recovery = 101% Analysis Date = 05/07/13 Pct Recovery = 101% Analysis Date = 05/07/13 Pct Recovery = 101% Analysis Date = 04/28/13 Pct Recovery = 101% Analysis Date = 04/28/13 Pct Recovery = 101% Analysis Date = 04/19/13 Pct Recovery = 102% Analysis Date = 04/19/13 Pct Recovery = 102% Analysis Date = 04/09/13 Pct Recovery = 102% Analysis Date = 04/09/13 Pct Recovery = 102% Analysis Date = 03/31/13 Pct Recovery = 102% Analysis Date = 03/31/13 Pct Recovery = 102% Analysis Date = 03/21/13 Pct Recovery = 102% Analysis Date = 03/21/13 Pct Recovery = 102% Analysis Date = 03/12/13 Pct Recovery = 102% Analysis Date = 03/12/13 Pct Recovery = 102% Analysis Date = 03/03/13 Pct Recovery = 103% Analysis Date = 03/03/13 Pct Recovery = 103% Analysis Date = 02/21/13 Pct Recovery = 103% Analysis Date = 02/21/13 Pct Recovery = 103% Analysis Date = 02/12/13 Pct Recovery = 103% Analysis Date = 02/12/13 Pct Recovery = 103% Analysis Date = 02/02/13 Pct Recovery = 103% Analysis Date = 02/02/13 Pct Recovery = 103% Analysis Date = 01/24/13 Pct Recovery = 104% Analysis Date = 01/24/13 Pct Recovery = 104% Analysis Date = 01/15/13 Pct Recovery = 104% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
DIAZINON

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 80 95% 13% 95% 12%
Total 80 95% 13% 95% 12%

Sample Statistics
DIAZINON

Characteristic N % % Basis
Plotted 80 100% Spiked
Estimated Values 1 1% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 80 .  
False Negatives 0 0% 0 out of 80
Not Spiked 38 .  
False Positives 3 8% 3 out of 38

OBSP Determination:
DIAZINON, OXYGEN ANALOG
METHOD: 2033 , TESTIDCODE: 61638GCM14

Laboratory ID = 20140100085 Lab Value = 0.155 Expected Conc. = 0.14 Report level label = 0.012 Pct Recovery = 111% Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl SpecificMix = T1130514013 Laboratory ID = 20132490342 Lab Value = 0.118 Expected Conc. = 0.14 Report level label = 0.012 Pct Recovery = 84% Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl SpecificMix = T1130514013 Laboratory ID = 20140230082 Lab Value = 0.100 Expected Conc. = 0.125 Report level label = 0.012 Pct Recovery = 80% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl SpecificMix = A093651 Laboratory ID = 20132420001 Lab Value = 0.104 Expected Conc. = 0.125 Report level label = 0.012 Pct Recovery = 83% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl SpecificMix = A093651 Laboratory ID = 20130810108 Lab Value = 0.111 Expected Conc. = 0.125 Report level label = 0.012 Pct Recovery = 89% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl SpecificMix = T1120530013 Laboratory ID = 20123560092 Lab Value = 0.073 Expected Conc. = 0.125 Report level label = 0.012 Pct Recovery = 59% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = T1120530013 Laboratory ID = 20162860079 Lab Value = 0.092 Expected Conc. = 0.075 Report level label = 0.012 Pct Recovery = 122% Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl SpecificMix = 060916 Laboratory ID = 20163150006 Lab Value = 0.093 Expected Conc. = 0.075 Report level label = 0.012 Pct Recovery = 124% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl SpecificMix = 060916 Laboratory ID = 20152460215 Lab Value = 0.063 Expected Conc. = 0.072 Report level label = 0.012 Pct Recovery = 88% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl SpecificMix = EN150514012 Laboratory ID = 20131370001 Lab Value = 0.089 Expected Conc. = 0.071 Report level label = 0.012 Pct Recovery = 126% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl SpecificMix = 1473000 Laboratory ID = 20140370077 Lab Value = 0.062 Expected Conc. = 0.07 Report level label = 0.012 Pct Recovery = 88% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl SpecificMix = T1130514013 Laboratory ID = 20132690010 Lab Value = 0.089 Expected Conc. = 0.07 Report level label = 0.012 Pct Recovery = 126% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl SpecificMix = T1130514013 Laboratory ID = 20171380001 Lab Value = 0.060 Expected Conc. = 0.0608 Report level label = 0.012 Pct Recovery = 99% Analysis Date = 06/07/17 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 041816 Laboratory ID = 20170740063 Lab Value = 0.073 Expected Conc. = 0.0608 Report level label = 0.012 Pct Recovery = 120% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl SpecificMix = 041816 Laboratory ID = 20161740258 Lab Value = 0.058 Expected Conc. = 0.0608 Report level label = 0.012 Pct Recovery = 96% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 041816 Laboratory ID = 20171660002 Lab Value = 0.082 Expected Conc. = 0.06 Report level label = 0.012 Pct Recovery = 137% Analysis Date = 08/23/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = 060916 Laboratory ID = 20170190026 Lab Value = 0.061 Expected Conc. = 0.06 Report level label = 0.012 Pct Recovery = 101% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = 060916 Laboratory ID = 20140860102 Lab Value = 0.049 Expected Conc. = 0.05 Report level label = 0.012 Pct Recovery = 98% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl SpecificMix = A093651 Laboratory ID = 20133400002 Lab Value = 0.047 Expected Conc. = 0.05 Report level label = 0.012 Pct Recovery = 94% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = A093651 Laboratory ID = 20132910008 Lab Value = 0.044 Expected Conc. = 0.05 Report level label = 0.012 Pct Recovery = 89% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = A093651 Laboratory ID = 20131920149 Lab Value = 0.046 Expected Conc. = 0.05 Report level label = 0.012 Pct Recovery = 92% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl SpecificMix = A093651 Laboratory ID = 20130390105 Lab Value = 0.043 Expected Conc. = 0.05 Report level label = 0.012 Pct Recovery = 85% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl SpecificMix = T1120530013 Laboratory ID = 20150720069 Lab Value = 0.033 Expected Conc. = 0.048 Report level label = 0.012 Pct Recovery = 69% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 03DD006 Laboratory ID = 20143110108 Lab Value = 0.036 Expected Conc. = 0.048 Report level label = 0.012 Pct Recovery = 74% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 03DD006 Laboratory ID = 20142960086 Lab Value = 0.032 Expected Conc. = 0.048 Report level label = 0.012 Pct Recovery = 67% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 03DD006 Laboratory ID = 20142270001 Lab Value = 0.034 Expected Conc. = 0.048 Report level label = 0.012 Pct Recovery = 71% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl SpecificMix = 03DD006 Laboratory ID = 20142720002 Lab Value = 0.046 Expected Conc. = 0.0479 Report level label = 0.012 Pct Recovery = 96% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl SpecificMix = LC06435 Laboratory ID = 20142530087 Lab Value = 0.046 Expected Conc. = 0.0479 Report level label = 0.012 Pct Recovery = 95% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl SpecificMix = LC06435 Laboratory ID = 20141570088 Lab Value = 0.062 Expected Conc. = 0.0479 Report level label = 0.012 Pct Recovery = 130% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl SpecificMix = LC06435 Laboratory ID = 20141220025 Lab Value = 0.058 Expected Conc. = 0.0479 Report level label = 0.012 Pct Recovery = 121% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl SpecificMix = LC06435 Laboratory ID = 20172230001 Lab Value = 0.064 Expected Conc. = 0.04 Report level label = 0.012 Pct Recovery = 160% Analysis Date = 10/19/17 SpikeMix = ChemService 6472100: 50 µl & Abs 071717Pest: 50 µl SpecificMix = 6472100 Laboratory ID = 20172560101 Lab Value = 0.033 Expected Conc. = 0.0393 Report level label = 0.012 Pct Recovery = 85% Analysis Date = 12/22/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6567600: 50 µl SpecificMix = EN170808006 Laboratory ID = 20172370001 Lab Value = 0.050 Expected Conc. = 0.0393 Report level label = 0.012 Pct Recovery = 126% Analysis Date = 11/18/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6537100: 50 µl SpecificMix = EN170808006 Laboratory ID = 20160630046 Lab Value = 0.037 Expected Conc. = 0.036 Report level label = 0.012 Pct Recovery = 102% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = EN150514012 Laboratory ID = 20153440001 Lab Value = 0.028 Expected Conc. = 0.036 Report level label = 0.012 Pct Recovery = 79% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = EN150514012 Laboratory ID = 20152330039 Lab Value = 0.041 Expected Conc. = 0.036 Report level label = 0.012 Pct Recovery = 114% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl SpecificMix = 041415 Laboratory ID = 20151900132 Lab Value = 0.056 Expected Conc. = 0.036 Report level label = 0.012 Pct Recovery = 155% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl SpecificMix = 041415 Laboratory ID = 20151270112 Lab Value = 0.052 Expected Conc. = 0.036 Report level label = 0.012 Pct Recovery = 144% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl SpecificMix = 041415 Laboratory ID = 20171940002 Lab Value = 0.050 Expected Conc. = 0.0304 Report level label = 0.012 Pct Recovery = 165% Analysis Date = 11/10/17 SpikeMix = ChemService 5054800: 40 µl & NSI 041816: 40 µl SpecificMix = 041816 Laboratory ID = 20162020124 Lab Value = 0.036 Expected Conc. = 0.0304 Report level label = 0.012 Pct Recovery = 119% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl SpecificMix = 041816 Laboratory ID = 20161600087 Lab Value = 0.046 Expected Conc. = 0.0304 Report level label = 0.012 Pct Recovery = 152% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 041816 Laboratory ID = 20161340228 Lab Value = 0.031 Expected Conc. = 0.0304 Report level label = 0.012 Pct Recovery = 102% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl SpecificMix = 041816 Laboratory ID = 20161190075 Lab Value = 0.032 Expected Conc. = 0.0304 Report level label = 0.012 Pct Recovery = 106% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 041816 Laboratory ID = 20171160110 Lab Value = 0.034 Expected Conc. = 0.03 Report level label = 0.012 Pct Recovery = 112% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = 060916 Laboratory ID = 20162520001 Lab Value = 0.055 Expected Conc. = 0.03 Report level label = 0.012 Pct Recovery = 182% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl SpecificMix = 060916 Laboratory ID = 20163560019 Lab Value = 0.038 Expected Conc. = 0.03 Report level label = 0.012 Pct Recovery = 125% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl SpecificMix = 060916 Laboratory ID = 20162380004 Lab Value = 0.043 Expected Conc. = 0.03 Report level label = 0.012 Pct Recovery = 144% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = 060916 Laboratory ID = 20140730138 Lab Value = 0.038 Expected Conc. = 0.0284 Report level label = 0.012 Pct Recovery = 132% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 1473000 Laboratory ID = 20133470008 Lab Value = 0.032 Expected Conc. = 0.0284 Report level label = 0.012 Pct Recovery = 114% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl SpecificMix = 1473000 Laboratory ID = 20133310030 Lab Value = 0.047 Expected Conc. = 0.0284 Report level label = 0.012 Pct Recovery = 164% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl SpecificMix = 1473000 Laboratory ID = 20131790009 Lab Value = 0.042 Expected Conc. = 0.0284 Report level label = 0.012 Pct Recovery = 147% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl SpecificMix = 1473000 Laboratory ID = 20131650073 Lab Value = 0.042 Expected Conc. = 0.0284 Report level label = 0.012 Pct Recovery = 148% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl SpecificMix = 1473000 Laboratory ID = 20133050050 Lab Value = 0.039 Expected Conc. = 0.028 Report level label = 0.012 Pct Recovery = 140% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl SpecificMix = T1130514013 Laboratory ID = 20132280016 Lab Value = 0.035 Expected Conc. = 0.028 Report level label = 0.012 Pct Recovery = 124% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl SpecificMix = T1130514013 Laboratory ID = 20173120093 Lab Value = 0.030 Expected Conc. = 0.024 Report level label = 0.012 Pct Recovery = 123% Analysis Date = 03/10/18 SpikeMix = ChemService 6472100: 30 µl & ChemService 6537100: 30 µl SpecificMix = 6472100 Laboratory ID = 20142200164 Lab Value = 0.020 Expected Conc. = 0.024 Report level label = 0.012 Pct Recovery = 81% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 03DD006 Laboratory ID = 20141420140 Lab Value = 0.020 Expected Conc. = 0.024 Report level label = 0.012 Pct Recovery = 84% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 03DD006 Laboratory ID = 20141080004 Lab Value = 0.019 Expected Conc. = 0.024 Report level label = 0.012 Pct Recovery = 77% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl SpecificMix = 03DD006 Laboratory ID = 20150150115 Lab Value = 0.028 Expected Conc. = 0.0239 Report level label = 0.012 Pct Recovery = 117% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl SpecificMix = LC06435 Laboratory ID = 20143370094 Lab Value = 0.023 Expected Conc. = 0.0239 Report level label = 0.012 Pct Recovery = 97% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl SpecificMix = LC06435 Laboratory ID = 20141910243 Lab Value = 0.023 Expected Conc. = 0.0239 Report level label = 0.012 Pct Recovery = 94% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = LC06435 Laboratory ID = 20141840097 Lab Value = 0.026 Expected Conc. = 0.0239 Report level label = 0.012 Pct Recovery = 109% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl SpecificMix = LC06435 Laboratory ID = 20161050143 Lab Value = 0.024 Expected Conc. = 0.018 Report level label = 0.012 Pct Recovery = 132% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 041415 Laboratory ID = 20160560044 Lab Value = 0.019 Expected Conc. = 0.018 Report level label = 0.012 Pct Recovery = 103% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl SpecificMix = 041415 Laboratory ID = 20160210080 Lab Value = 0.016 Expected Conc. = 0.018 Report level label = 0.012 Pct Recovery = 89% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 041415 Laboratory ID = 20160070059 Lab Value = 0.017 Expected Conc. = 0.018 Report level label = 0.012 Pct Recovery = 95% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = EN150514012 Laboratory ID = 20153160001 Lab Value = 0.014 Expected Conc. = 0.018 Report level label = 0.012 Pct Recovery = 77% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = EN150514012 Laboratory ID = 20152950078 Lab Value = 0.012 Expected Conc. = 0.018 Report level label = 0.012 Pct Recovery = 65% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 041415 Laboratory ID = 20152040177 Lab Value = 0.035 Expected Conc. = 0.018 Report level label = 0.012 Pct Recovery = 196% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl SpecificMix = 041415 Laboratory ID = 20151480170 Lab Value = 0.024 Expected Conc. = 0.018 Report level label = 0.012 Pct Recovery = 133% Analysis Date = 06/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150514012 Laboratory ID = 20151210037 Lab Value = 0.028 Expected Conc. = 0.018 Report level label = 0.012 Pct Recovery = 156% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 041415 Analysis Date = 03/10/18 Pct Recovery = 134% Analysis Date = 02/28/18 Pct Recovery = 134% Analysis Date = 02/28/18 Pct Recovery = 134% Analysis Date = 02/19/18 Pct Recovery = 134% Analysis Date = 02/19/18 Pct Recovery = 134% Analysis Date = 02/09/18 Pct Recovery = 134% Analysis Date = 02/09/18 Pct Recovery = 134% Analysis Date = 01/31/18 Pct Recovery = 133% Analysis Date = 01/31/18 Pct Recovery = 133% Analysis Date = 01/22/18 Pct Recovery = 133% Analysis Date = 01/22/18 Pct Recovery = 133% Analysis Date = 01/12/18 Pct Recovery = 133% Analysis Date = 01/12/18 Pct Recovery = 133% Analysis Date = 01/03/18 Pct Recovery = 132% Analysis Date = 01/03/18 Pct Recovery = 132% Analysis Date = 12/24/17 Pct Recovery = 132% Analysis Date = 12/24/17 Pct Recovery = 132% Analysis Date = 12/15/17 Pct Recovery = 132% Analysis Date = 12/15/17 Pct Recovery = 132% Analysis Date = 12/06/17 Pct Recovery = 131% Analysis Date = 12/06/17 Pct Recovery = 131% Analysis Date = 11/26/17 Pct Recovery = 131% Analysis Date = 11/26/17 Pct Recovery = 131% Analysis Date = 11/17/17 Pct Recovery = 131% Analysis Date = 11/17/17 Pct Recovery = 131% Analysis Date = 11/07/17 Pct Recovery = 130% Analysis Date = 11/07/17 Pct Recovery = 130% Analysis Date = 10/29/17 Pct Recovery = 130% Analysis Date = 10/29/17 Pct Recovery = 130% Analysis Date = 10/20/17 Pct Recovery = 130% Analysis Date = 10/20/17 Pct Recovery = 130% Analysis Date = 10/10/17 Pct Recovery = 130% Analysis Date = 10/10/17 Pct Recovery = 130% Analysis Date = 10/01/17 Pct Recovery = 129% Analysis Date = 10/01/17 Pct Recovery = 129% Analysis Date = 09/21/17 Pct Recovery = 129% Analysis Date = 09/21/17 Pct Recovery = 129% Analysis Date = 09/12/17 Pct Recovery = 129% Analysis Date = 09/12/17 Pct Recovery = 129% Analysis Date = 09/03/17 Pct Recovery = 128% Analysis Date = 09/03/17 Pct Recovery = 128% Analysis Date = 08/24/17 Pct Recovery = 128% Analysis Date = 08/24/17 Pct Recovery = 128% Analysis Date = 08/15/17 Pct Recovery = 128% Analysis Date = 08/15/17 Pct Recovery = 128% Analysis Date = 08/05/17 Pct Recovery = 127% Analysis Date = 08/05/17 Pct Recovery = 127% Analysis Date = 07/27/17 Pct Recovery = 127% Analysis Date = 07/27/17 Pct Recovery = 127% Analysis Date = 07/18/17 Pct Recovery = 127% Analysis Date = 07/18/17 Pct Recovery = 127% Analysis Date = 07/08/17 Pct Recovery = 126% Analysis Date = 07/08/17 Pct Recovery = 126% Analysis Date = 06/29/17 Pct Recovery = 126% Analysis Date = 06/29/17 Pct Recovery = 126% Analysis Date = 06/19/17 Pct Recovery = 126% Analysis Date = 06/19/17 Pct Recovery = 126% Analysis Date = 06/10/17 Pct Recovery = 125% Analysis Date = 06/10/17 Pct Recovery = 125% Analysis Date = 06/01/17 Pct Recovery = 125% Analysis Date = 06/01/17 Pct Recovery = 125% Analysis Date = 05/22/17 Pct Recovery = 125% Analysis Date = 05/22/17 Pct Recovery = 125% Analysis Date = 05/13/17 Pct Recovery = 125% Analysis Date = 05/13/17 Pct Recovery = 125% Analysis Date = 05/03/17 Pct Recovery = 124% Analysis Date = 05/03/17 Pct Recovery = 124% Analysis Date = 04/24/17 Pct Recovery = 124% Analysis Date = 04/24/17 Pct Recovery = 124% Analysis Date = 04/15/17 Pct Recovery = 124% Analysis Date = 04/15/17 Pct Recovery = 124% Analysis Date = 04/05/17 Pct Recovery = 123% Analysis Date = 04/05/17 Pct Recovery = 123% Analysis Date = 03/27/17 Pct Recovery = 123% Analysis Date = 03/27/17 Pct Recovery = 123% Analysis Date = 03/17/17 Pct Recovery = 123% Analysis Date = 03/17/17 Pct Recovery = 123% Analysis Date = 03/08/17 Pct Recovery = 122% Analysis Date = 03/08/17 Pct Recovery = 122% Analysis Date = 02/27/17 Pct Recovery = 122% Analysis Date = 02/27/17 Pct Recovery = 122% Analysis Date = 02/17/17 Pct Recovery = 122% Analysis Date = 02/17/17 Pct Recovery = 122% Analysis Date = 02/08/17 Pct Recovery = 122% Analysis Date = 02/08/17 Pct Recovery = 122% Analysis Date = 01/29/17 Pct Recovery = 121% Analysis Date = 01/29/17 Pct Recovery = 121% Analysis Date = 01/20/17 Pct Recovery = 121% Analysis Date = 01/20/17 Pct Recovery = 121% Analysis Date = 01/11/17 Pct Recovery = 121% Analysis Date = 01/11/17 Pct Recovery = 121% Analysis Date = 01/01/17 Pct Recovery = 121% Analysis Date = 01/01/17 Pct Recovery = 121% Analysis Date = 12/23/16 Pct Recovery = 120% Analysis Date = 12/23/16 Pct Recovery = 120% Analysis Date = 12/13/16 Pct Recovery = 120% Analysis Date = 12/13/16 Pct Recovery = 120% Analysis Date = 12/04/16 Pct Recovery = 120% Analysis Date = 12/04/16 Pct Recovery = 120% Analysis Date = 11/25/16 Pct Recovery = 120% Analysis Date = 11/25/16 Pct Recovery = 120% Analysis Date = 11/15/16 Pct Recovery = 119% Analysis Date = 11/15/16 Pct Recovery = 119% Analysis Date = 11/06/16 Pct Recovery = 119% Analysis Date = 11/06/16 Pct Recovery = 119% Analysis Date = 10/27/16 Pct Recovery = 119% Analysis Date = 10/27/16 Pct Recovery = 119% Analysis Date = 10/18/16 Pct Recovery = 119% Analysis Date = 10/18/16 Pct Recovery = 119% Analysis Date = 10/09/16 Pct Recovery = 118% Analysis Date = 10/09/16 Pct Recovery = 118% Analysis Date = 09/29/16 Pct Recovery = 118% Analysis Date = 09/29/16 Pct Recovery = 118% Analysis Date = 09/20/16 Pct Recovery = 118% Analysis Date = 09/20/16 Pct Recovery = 118% Analysis Date = 09/10/16 Pct Recovery = 118% Analysis Date = 09/10/16 Pct Recovery = 118% Analysis Date = 09/01/16 Pct Recovery = 117% Analysis Date = 09/01/16 Pct Recovery = 117% Analysis Date = 08/23/16 Pct Recovery = 117% Analysis Date = 08/23/16 Pct Recovery = 117% Analysis Date = 08/13/16 Pct Recovery = 117% Analysis Date = 08/13/16 Pct Recovery = 117% Analysis Date = 08/04/16 Pct Recovery = 117% Analysis Date = 08/04/16 Pct Recovery = 117% Analysis Date = 07/25/16 Pct Recovery = 116% Analysis Date = 07/25/16 Pct Recovery = 116% Analysis Date = 07/16/16 Pct Recovery = 116% Analysis Date = 07/16/16 Pct Recovery = 116% Analysis Date = 07/07/16 Pct Recovery = 116% Analysis Date = 07/07/16 Pct Recovery = 116% Analysis Date = 06/27/16 Pct Recovery = 116% Analysis Date = 06/27/16 Pct Recovery = 116% Analysis Date = 06/18/16 Pct Recovery = 116% Analysis Date = 06/18/16 Pct Recovery = 116% Analysis Date = 06/08/16 Pct Recovery = 115% Analysis Date = 06/08/16 Pct Recovery = 115% Analysis Date = 05/30/16 Pct Recovery = 115% Analysis Date = 05/30/16 Pct Recovery = 115% Analysis Date = 05/21/16 Pct Recovery = 115% Analysis Date = 05/21/16 Pct Recovery = 115% Analysis Date = 05/11/16 Pct Recovery = 115% Analysis Date = 05/11/16 Pct Recovery = 115% Analysis Date = 05/02/16 Pct Recovery = 115% Analysis Date = 05/02/16 Pct Recovery = 115% Analysis Date = 04/22/16 Pct Recovery = 115% Analysis Date = 04/22/16 Pct Recovery = 115% Analysis Date = 04/13/16 Pct Recovery = 114% Analysis Date = 04/13/16 Pct Recovery = 114% Analysis Date = 04/04/16 Pct Recovery = 114% Analysis Date = 04/04/16 Pct Recovery = 114% Analysis Date = 03/25/16 Pct Recovery = 114% Analysis Date = 03/25/16 Pct Recovery = 114% Analysis Date = 03/16/16 Pct Recovery = 114% Analysis Date = 03/16/16 Pct Recovery = 114% Analysis Date = 03/06/16 Pct Recovery = 114% Analysis Date = 03/06/16 Pct Recovery = 114% Analysis Date = 02/26/16 Pct Recovery = 114% Analysis Date = 02/26/16 Pct Recovery = 114% Analysis Date = 02/17/16 Pct Recovery = 113% Analysis Date = 02/17/16 Pct Recovery = 113% Analysis Date = 02/07/16 Pct Recovery = 113% Analysis Date = 02/07/16 Pct Recovery = 113% Analysis Date = 01/29/16 Pct Recovery = 113% Analysis Date = 01/29/16 Pct Recovery = 113% Analysis Date = 01/19/16 Pct Recovery = 113% Analysis Date = 01/19/16 Pct Recovery = 113% Analysis Date = 01/10/16 Pct Recovery = 112% Analysis Date = 01/10/16 Pct Recovery = 112% Analysis Date = 01/01/16 Pct Recovery = 112% Analysis Date = 01/01/16 Pct Recovery = 112% Analysis Date = 12/22/15 Pct Recovery = 112% Analysis Date = 12/22/15 Pct Recovery = 112% Analysis Date = 12/13/15 Pct Recovery = 111% Analysis Date = 12/13/15 Pct Recovery = 111% Analysis Date = 12/03/15 Pct Recovery = 111% Analysis Date = 12/03/15 Pct Recovery = 111% Analysis Date = 11/24/15 Pct Recovery = 111% Analysis Date = 11/24/15 Pct Recovery = 111% Analysis Date = 11/15/15 Pct Recovery = 111% Analysis Date = 11/15/15 Pct Recovery = 111% Analysis Date = 11/05/15 Pct Recovery = 110% Analysis Date = 11/05/15 Pct Recovery = 110% Analysis Date = 10/27/15 Pct Recovery = 110% Analysis Date = 10/27/15 Pct Recovery = 110% Analysis Date = 10/17/15 Pct Recovery = 110% Analysis Date = 10/17/15 Pct Recovery = 110% Analysis Date = 10/08/15 Pct Recovery = 109% Analysis Date = 10/08/15 Pct Recovery = 109% Analysis Date = 09/29/15 Pct Recovery = 109% Analysis Date = 09/29/15 Pct Recovery = 109% Analysis Date = 09/19/15 Pct Recovery = 109% Analysis Date = 09/19/15 Pct Recovery = 109% Analysis Date = 09/10/15 Pct Recovery = 109% Analysis Date = 09/10/15 Pct Recovery = 109% Analysis Date = 08/31/15 Pct Recovery = 108% Analysis Date = 08/31/15 Pct Recovery = 108% Analysis Date = 08/22/15 Pct Recovery = 108% Analysis Date = 08/22/15 Pct Recovery = 108% Analysis Date = 08/13/15 Pct Recovery = 108% Analysis Date = 08/13/15 Pct Recovery = 108% Analysis Date = 08/03/15 Pct Recovery = 107% Analysis Date = 08/03/15 Pct Recovery = 107% Analysis Date = 07/25/15 Pct Recovery = 107% Analysis Date = 07/25/15 Pct Recovery = 107% Analysis Date = 07/15/15 Pct Recovery = 107% Analysis Date = 07/15/15 Pct Recovery = 107% Analysis Date = 07/06/15 Pct Recovery = 107% Analysis Date = 07/06/15 Pct Recovery = 107% Analysis Date = 06/27/15 Pct Recovery = 107% Analysis Date = 06/27/15 Pct Recovery = 107% Analysis Date = 06/17/15 Pct Recovery = 107% Analysis Date = 06/17/15 Pct Recovery = 107% Analysis Date = 06/08/15 Pct Recovery = 107% Analysis Date = 06/08/15 Pct Recovery = 107% Analysis Date = 05/29/15 Pct Recovery = 107% Analysis Date = 05/29/15 Pct Recovery = 107% Analysis Date = 05/20/15 Pct Recovery = 107% Analysis Date = 05/20/15 Pct Recovery = 107% Analysis Date = 05/11/15 Pct Recovery = 107% Analysis Date = 05/11/15 Pct Recovery = 107% Analysis Date = 05/01/15 Pct Recovery = 107% Analysis Date = 05/01/15 Pct Recovery = 107% Analysis Date = 04/22/15 Pct Recovery = 107% Analysis Date = 04/22/15 Pct Recovery = 107% Analysis Date = 04/12/15 Pct Recovery = 107% Analysis Date = 04/12/15 Pct Recovery = 107% Analysis Date = 04/03/15 Pct Recovery = 107% Analysis Date = 04/03/15 Pct Recovery = 107% Analysis Date = 03/25/15 Pct Recovery = 107% Analysis Date = 03/25/15 Pct Recovery = 107% Analysis Date = 03/15/15 Pct Recovery = 107% Analysis Date = 03/15/15 Pct Recovery = 107% Analysis Date = 03/06/15 Pct Recovery = 107% Analysis Date = 03/06/15 Pct Recovery = 107% Analysis Date = 02/24/15 Pct Recovery = 107% Analysis Date = 02/24/15 Pct Recovery = 107% Analysis Date = 02/15/15 Pct Recovery = 107% Analysis Date = 02/15/15 Pct Recovery = 107% Analysis Date = 02/06/15 Pct Recovery = 107% Analysis Date = 02/06/15 Pct Recovery = 107% Analysis Date = 01/27/15 Pct Recovery = 107% Analysis Date = 01/27/15 Pct Recovery = 107% Analysis Date = 01/18/15 Pct Recovery = 107% Analysis Date = 01/18/15 Pct Recovery = 107% Analysis Date = 01/08/15 Pct Recovery = 107% Analysis Date = 01/08/15 Pct Recovery = 107% Analysis Date = 12/30/14 Pct Recovery = 107% Analysis Date = 12/30/14 Pct Recovery = 107% Analysis Date = 12/21/14 Pct Recovery = 107% Analysis Date = 12/21/14 Pct Recovery = 107% Analysis Date = 12/11/14 Pct Recovery = 107% Analysis Date = 12/11/14 Pct Recovery = 107% Analysis Date = 12/02/14 Pct Recovery = 107% Analysis Date = 12/02/14 Pct Recovery = 107% Analysis Date = 11/22/14 Pct Recovery = 107% Analysis Date = 11/22/14 Pct Recovery = 107% Analysis Date = 11/13/14 Pct Recovery = 107% Analysis Date = 11/13/14 Pct Recovery = 107% Analysis Date = 11/04/14 Pct Recovery = 107% Analysis Date = 11/04/14 Pct Recovery = 107% Analysis Date = 10/25/14 Pct Recovery = 107% Analysis Date = 10/25/14 Pct Recovery = 107% Analysis Date = 10/16/14 Pct Recovery = 107% Analysis Date = 10/16/14 Pct Recovery = 107% Analysis Date = 10/06/14 Pct Recovery = 106% Analysis Date = 10/06/14 Pct Recovery = 106% Analysis Date = 09/27/14 Pct Recovery = 106% Analysis Date = 09/27/14 Pct Recovery = 106% Analysis Date = 09/18/14 Pct Recovery = 106% Analysis Date = 09/18/14 Pct Recovery = 106% Analysis Date = 09/08/14 Pct Recovery = 105% Analysis Date = 09/08/14 Pct Recovery = 105% Analysis Date = 08/30/14 Pct Recovery = 105% Analysis Date = 08/30/14 Pct Recovery = 105% Analysis Date = 08/20/14 Pct Recovery = 105% Analysis Date = 08/20/14 Pct Recovery = 105% Analysis Date = 08/11/14 Pct Recovery = 105% Analysis Date = 08/11/14 Pct Recovery = 105% Analysis Date = 08/02/14 Pct Recovery = 104% Analysis Date = 08/02/14 Pct Recovery = 104% Analysis Date = 07/23/14 Pct Recovery = 104% Analysis Date = 07/23/14 Pct Recovery = 104% Analysis Date = 07/14/14 Pct Recovery = 104% Analysis Date = 07/14/14 Pct Recovery = 104% Analysis Date = 07/04/14 Pct Recovery = 103% Analysis Date = 07/04/14 Pct Recovery = 103% Analysis Date = 06/25/14 Pct Recovery = 103% Analysis Date = 06/25/14 Pct Recovery = 103% Analysis Date = 06/16/14 Pct Recovery = 103% Analysis Date = 06/16/14 Pct Recovery = 103% Analysis Date = 06/06/14 Pct Recovery = 103% Analysis Date = 06/06/14 Pct Recovery = 103% Analysis Date = 05/28/14 Pct Recovery = 102% Analysis Date = 05/28/14 Pct Recovery = 102% Analysis Date = 05/18/14 Pct Recovery = 102% Analysis Date = 05/18/14 Pct Recovery = 102% Analysis Date = 05/09/14 Pct Recovery = 102% Analysis Date = 05/09/14 Pct Recovery = 102% Analysis Date = 04/30/14 Pct Recovery = 103% Analysis Date = 04/30/14 Pct Recovery = 103% Analysis Date = 04/20/14 Pct Recovery = 103% Analysis Date = 04/20/14 Pct Recovery = 103% Analysis Date = 04/11/14 Pct Recovery = 103% Analysis Date = 04/11/14 Pct Recovery = 103% Analysis Date = 04/01/14 Pct Recovery = 103% Analysis Date = 04/01/14 Pct Recovery = 103% Analysis Date = 03/23/14 Pct Recovery = 103% Analysis Date = 03/23/14 Pct Recovery = 103% Analysis Date = 03/14/14 Pct Recovery = 104% Analysis Date = 03/14/14 Pct Recovery = 104% Analysis Date = 03/04/14 Pct Recovery = 104% Analysis Date = 03/04/14 Pct Recovery = 104% Analysis Date = 02/23/14 Pct Recovery = 104% Analysis Date = 02/23/14 Pct Recovery = 104% Analysis Date = 02/13/14 Pct Recovery = 104% Analysis Date = 02/13/14 Pct Recovery = 104% Analysis Date = 02/04/14 Pct Recovery = 105% Analysis Date = 02/04/14 Pct Recovery = 105% Analysis Date = 01/26/14 Pct Recovery = 105% Analysis Date = 01/26/14 Pct Recovery = 105% Analysis Date = 01/16/14 Pct Recovery = 105% Analysis Date = 01/16/14 Pct Recovery = 105% Analysis Date = 01/07/14 Pct Recovery = 105% Analysis Date = 01/07/14 Pct Recovery = 105% Analysis Date = 12/28/13 Pct Recovery = 105% Analysis Date = 12/28/13 Pct Recovery = 105% Analysis Date = 12/19/13 Pct Recovery = 105% Analysis Date = 12/19/13 Pct Recovery = 105% Analysis Date = 12/10/13 Pct Recovery = 105% Analysis Date = 12/10/13 Pct Recovery = 105% Analysis Date = 11/30/13 Pct Recovery = 106% Analysis Date = 11/30/13 Pct Recovery = 106% Analysis Date = 11/21/13 Pct Recovery = 106% Analysis Date = 11/21/13 Pct Recovery = 106% Analysis Date = 11/11/13 Pct Recovery = 106% Analysis Date = 11/11/13 Pct Recovery = 106% Analysis Date = 11/02/13 Pct Recovery = 106% Analysis Date = 11/02/13 Pct Recovery = 106% Analysis Date = 10/24/13 Pct Recovery = 106% Analysis Date = 10/24/13 Pct Recovery = 106% Analysis Date = 10/14/13 Pct Recovery = 106% Analysis Date = 10/14/13 Pct Recovery = 106% Analysis Date = 10/05/13 Pct Recovery = 106% Analysis Date = 10/05/13 Pct Recovery = 106% Analysis Date = 09/25/13 Pct Recovery = 106% Analysis Date = 09/25/13 Pct Recovery = 106% Analysis Date = 09/16/13 Pct Recovery = 106% Analysis Date = 09/16/13 Pct Recovery = 106% Analysis Date = 09/07/13 Pct Recovery = 106% Analysis Date = 09/07/13 Pct Recovery = 106% Analysis Date = 08/28/13 Pct Recovery = 106% Analysis Date = 08/28/13 Pct Recovery = 106% Analysis Date = 08/19/13 Pct Recovery = 106% Analysis Date = 08/19/13 Pct Recovery = 106% Analysis Date = 08/09/13 Pct Recovery = 107% Analysis Date = 08/09/13 Pct Recovery = 107% Analysis Date = 07/31/13 Pct Recovery = 107% Analysis Date = 07/31/13 Pct Recovery = 107% Analysis Date = 07/22/13 Pct Recovery = 107% Analysis Date = 07/22/13 Pct Recovery = 107% Analysis Date = 07/12/13 Pct Recovery = 107% Analysis Date = 07/12/13 Pct Recovery = 107% Analysis Date = 07/03/13 Pct Recovery = 107% Analysis Date = 07/03/13 Pct Recovery = 107% Analysis Date = 06/23/13 Pct Recovery = 107% Analysis Date = 06/23/13 Pct Recovery = 107% Analysis Date = 06/14/13 Pct Recovery = 107% Analysis Date = 06/14/13 Pct Recovery = 107% Analysis Date = 06/05/13 Pct Recovery = 107% Analysis Date = 06/05/13 Pct Recovery = 107% Analysis Date = 05/26/13 Pct Recovery = 107% Analysis Date = 05/26/13 Pct Recovery = 107% Analysis Date = 05/17/13 Pct Recovery = 107% Analysis Date = 05/17/13 Pct Recovery = 107% Analysis Date = 05/07/13 Pct Recovery = 107% Analysis Date = 05/07/13 Pct Recovery = 107% Analysis Date = 04/28/13 Pct Recovery = 107% Analysis Date = 04/28/13 Pct Recovery = 107% Analysis Date = 04/19/13 Pct Recovery = 107% Analysis Date = 04/19/13 Pct Recovery = 107% Analysis Date = 04/09/13 Pct Recovery = 107% Analysis Date = 04/09/13 Pct Recovery = 107% Analysis Date = 03/31/13 Pct Recovery = 107% Analysis Date = 03/31/13 Pct Recovery = 107% Analysis Date = 03/21/13 Pct Recovery = 107% Analysis Date = 03/21/13 Pct Recovery = 107% Analysis Date = 03/12/13 Pct Recovery = 107% Analysis Date = 03/12/13 Pct Recovery = 107% Analysis Date = 03/03/13 Pct Recovery = 108% Analysis Date = 03/03/13 Pct Recovery = 108% Analysis Date = 02/21/13 Pct Recovery = 108% Analysis Date = 02/21/13 Pct Recovery = 108% Analysis Date = 02/12/13 Pct Recovery = 108% Analysis Date = 02/12/13 Pct Recovery = 108% Analysis Date = 02/02/13 Pct Recovery = 108% Analysis Date = 02/02/13 Pct Recovery = 108% Analysis Date = 01/24/13 Pct Recovery = 108% Analysis Date = 01/24/13 Pct Recovery = 108% Analysis Date = 01/15/13 Pct Recovery = 108% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
DIAZINON, OXYGEN ANALOG

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 71 111% 30% 106% 31%
Total 71 111% 30% 106% 31%

Sample Statistics
DIAZINON, OXYGEN ANALOG

Characteristic N % % Basis
Plotted 71 96% Spiked
Estimated Values 7 9% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 1 1% Spiked
Spiked 74 .  
False Negatives 2 3% 2 out of 74
Not Spiked 41 .  
False Positives 0 0% 0 out of 41

OBSP Determination:
DICHLOROVOS (DICHLORVOS)
METHOD: 2033 , TESTIDCODE: 38775GCM39

Laboratory ID = 20140100085 Lab Value = 0.270 Expected Conc. = 0.401 Report level label = 0.04 Pct Recovery = 67% Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl SpecificMix = 042413 Laboratory ID = 20130250061 Lab Value = 0.140 Expected Conc. = 0.299 Report level label = 0.04 Pct Recovery = 47% Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl SpecificMix = 05BB029 Laboratory ID = 20172510330 Lab Value = 0.131 Expected Conc. = 0.268 Report level label = 0.04 Pct Recovery = 49% Analysis Date = 12/29/17 SpikeMix = ChemService 6537100: 100 µl & Abs 071817Pest: 100 µl SpecificMix = 071817Pest Laboratory ID = 20162860079 Lab Value = 0.124 Expected Conc. = 0.251 Report level label = 0.04 Pct Recovery = 49% Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl SpecificMix = 060916 Laboratory ID = 20163150006 Lab Value = 0.080 Expected Conc. = 0.251 Report level label = 0.04 Pct Recovery = 32% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl SpecificMix = 060916 Laboratory ID = 20152750006 Lab Value = 0.112 Expected Conc. = 0.24 Report level label = 0.04 Pct Recovery = 47% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl SpecificMix = EN150514012 Laboratory ID = 20152460215 Lab Value = 0.114 Expected Conc. = 0.24 Report level label = 0.04 Pct Recovery = 48% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl SpecificMix = EN150514012 Laboratory ID = 20171660002 Lab Value = 0.138 Expected Conc. = 0.2008 Report level label = 0.04 Pct Recovery = 69% Analysis Date = 08/23/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = 060916 Laboratory ID = 20170190026 Lab Value = 0.052 Expected Conc. = 0.2008 Report level label = 0.04 Pct Recovery = 26% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = 060916 Laboratory ID = 20132690010 Lab Value = 0.135 Expected Conc. = 0.2005 Report level label = 0.04 Pct Recovery = 67% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl SpecificMix = 042413 Laboratory ID = 20132560001 Lab Value = 0.091 Expected Conc. = 0.2005 Report level label = 0.04 Pct Recovery = 45% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl SpecificMix = 042413 Laboratory ID = 20171380001 Lab Value = 0.080 Expected Conc. = 0.2 Report level label = 0.04 Pct Recovery = 40% Analysis Date = 06/07/17 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 041816 Laboratory ID = 20170740063 Lab Value = 0.085 Expected Conc. = 0.2 Report level label = 0.04 Pct Recovery = 43% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl SpecificMix = 041816 Laboratory ID = 20161740258 Lab Value = 0.122 Expected Conc. = 0.2 Report level label = 0.04 Pct Recovery = 61% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 041816 Laboratory ID = 20132140002 Lab Value = 0.105 Expected Conc. = 0.199 Report level label = 0.04 Pct Recovery = 53% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl SpecificMix = 04CC101 Laboratory ID = 20150720069 Lab Value = 0.041 Expected Conc. = 0.1602 Report level label = 0.04 Pct Recovery = 26% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 0227-14-08 Laboratory ID = 20141770149 Lab Value = 0.084 Expected Conc. = 0.1602 Report level label = 0.04 Pct Recovery = 52% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl SpecificMix = 0227-14-08 Laboratory ID = 20141570088 Lab Value = 0.099 Expected Conc. = 0.1602 Report level label = 0.04 Pct Recovery = 62% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl SpecificMix = 0227-14-08 Laboratory ID = 20150430092 Lab Value = 0.065 Expected Conc. = 0.1578 Report level label = 0.04 Pct Recovery = 41% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl SpecificMix = 042814 Laboratory ID = 20143240095 Lab Value = 0.101 Expected Conc. = 0.1578 Report level label = 0.04 Pct Recovery = 64% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl SpecificMix = 042814 Laboratory ID = 20142960086 Lab Value = 0.077 Expected Conc. = 0.1578 Report level label = 0.04 Pct Recovery = 49% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 042814 Laboratory ID = 20142530087 Lab Value = 0.062 Expected Conc. = 0.1578 Report level label = 0.04 Pct Recovery = 39% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl SpecificMix = 042814 Laboratory ID = 20130940097 Lab Value = 0.098 Expected Conc. = 0.151 Report level label = 0.04 Pct Recovery = 65% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = 052412 Laboratory ID = 20130100066 Lab Value = 0.098 Expected Conc. = 0.151 Report level label = 0.04 Pct Recovery = 65% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl SpecificMix = 052412 Laboratory ID = 20140230082 Lab Value = 0.072 Expected Conc. = 0.1505 Report level label = 0.04 Pct Recovery = 48% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl SpecificMix = 012513 Laboratory ID = 20132420001 Lab Value = 0.099 Expected Conc. = 0.1505 Report level label = 0.04 Pct Recovery = 66% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl SpecificMix = 012513 Laboratory ID = 20172560101 Lab Value = 0.065 Expected Conc. = 0.135 Report level label = 0.04 Pct Recovery = 48% Analysis Date = 12/22/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6567600: 50 µl SpecificMix = 6567600 Laboratory ID = 20152330039 Lab Value = 0.082 Expected Conc. = 0.1208 Report level label = 0.04 Pct Recovery = 68% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl SpecificMix = 041415 Laboratory ID = 20151900132 Lab Value = 0.065 Expected Conc. = 0.1208 Report level label = 0.04 Pct Recovery = 54% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl SpecificMix = 041415 Laboratory ID = 20151270112 Lab Value = 0.091 Expected Conc. = 0.1208 Report level label = 0.04 Pct Recovery = 75% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl SpecificMix = 041415 Laboratory ID = 20160630046 Lab Value = 0.031 Expected Conc. = 0.12 Report level label = 0.04 Pct Recovery = 26% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = EN150514012 Laboratory ID = 20153440001 Lab Value = 0.044 Expected Conc. = 0.12 Report level label = 0.04 Pct Recovery = 37% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = EN150514012 Laboratory ID = 20171160110 Lab Value = 0.047 Expected Conc. = 0.1004 Report level label = 0.04 Pct Recovery = 47% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = 060916 Laboratory ID = 20162520001 Lab Value = 0.086 Expected Conc. = 0.1004 Report level label = 0.04 Pct Recovery = 86% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl SpecificMix = 060916 Laboratory ID = 20163560019 Lab Value = 0.122 Expected Conc. = 0.1004 Report level label = 0.04 Pct Recovery = 122% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl SpecificMix = 060916 Laboratory ID = 20162380004 Lab Value = 0.040 Expected Conc. = 0.1004 Report level label = 0.04 Pct Recovery = 40% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = 060916 Laboratory ID = 20171940002 Lab Value = 0.065 Expected Conc. = 0.1 Report level label = 0.04 Pct Recovery = 65% Analysis Date = 11/10/17 SpikeMix = ChemService 5054800: 40 µl & NSI 041816: 40 µl SpecificMix = 041816 Laboratory ID = 20162020124 Lab Value = 0.045 Expected Conc. = 0.1 Report level label = 0.04 Pct Recovery = 45% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl SpecificMix = 041816 Laboratory ID = 20161600087 Lab Value = 0.043 Expected Conc. = 0.1 Report level label = 0.04 Pct Recovery = 43% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 041816 Laboratory ID = 20161340228 Lab Value = 0.023 Expected Conc. = 0.1 Report level label = 0.04 Pct Recovery = 23% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl SpecificMix = 041816 Laboratory ID = 20161190075 Lab Value = 0.018 Expected Conc. = 0.1 Report level label = 0.04 Pct Recovery = 18% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 041816 Laboratory ID = 20172780018 Lab Value = 0.054 Expected Conc. = 0.0804 Report level label = 0.04 Pct Recovery = 67% Analysis Date = 02/08/18 SpikeMix = ChemService 6537100: 30 µl & Abs 071817Pest: 30 µl SpecificMix = 071817Pest Laboratory ID = 20133580036 Lab Value = 0.041 Expected Conc. = 0.0802 Report level label = 0.04 Pct Recovery = 51% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 042413 Laboratory ID = 20133190012 Lab Value = 0.077 Expected Conc. = 0.0802 Report level label = 0.04 Pct Recovery = 96% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 042413 Laboratory ID = 20131650073 Lab Value = 0.055 Expected Conc. = 0.0802 Report level label = 0.04 Pct Recovery = 69% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl SpecificMix = 042413 Laboratory ID = 20141840097 Lab Value = 0.031 Expected Conc. = 0.0801 Report level label = 0.04 Pct Recovery = 39% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20141490205 Lab Value = 0.064 Expected Conc. = 0.0801 Report level label = 0.04 Pct Recovery = 80% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20141420140 Lab Value = 0.038 Expected Conc. = 0.0801 Report level label = 0.04 Pct Recovery = 47% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20141360094 Lab Value = 0.050 Expected Conc. = 0.0801 Report level label = 0.04 Pct Recovery = 62% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20140730138 Lab Value = 0.026 Expected Conc. = 0.0796 Report level label = 0.04 Pct Recovery = 33% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 04CC101 Laboratory ID = 20140510043 Lab Value = 0.037 Expected Conc. = 0.0796 Report level label = 0.04 Pct Recovery = 46% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 04CC101 Laboratory ID = 20133310030 Lab Value = 0.074 Expected Conc. = 0.0796 Report level label = 0.04 Pct Recovery = 93% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl SpecificMix = 04CC101 Laboratory ID = 20132280016 Lab Value = 0.060 Expected Conc. = 0.0796 Report level label = 0.04 Pct Recovery = 75% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl SpecificMix = 04CC101 Laboratory ID = 20131510026 Lab Value = 0.054 Expected Conc. = 0.0796 Report level label = 0.04 Pct Recovery = 68% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl SpecificMix = 04CC101 Laboratory ID = 20143370094 Lab Value = 0.030 Expected Conc. = 0.0789 Report level label = 0.04 Pct Recovery = 38% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl SpecificMix = 042814 Laboratory ID = 20142820151 Lab Value = 0.043 Expected Conc. = 0.0789 Report level label = 0.04 Pct Recovery = 54% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl SpecificMix = 042814 Laboratory ID = 20142470041 Lab Value = 0.035 Expected Conc. = 0.0789 Report level label = 0.04 Pct Recovery = 44% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl SpecificMix = 042814 Laboratory ID = 20142200164 Lab Value = 0.056 Expected Conc. = 0.0789 Report level label = 0.04 Pct Recovery = 71% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 042814 Laboratory ID = 20161050143 Lab Value = 0.020 Expected Conc. = 0.0604 Report level label = 0.04 Pct Recovery = 33% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 041415 Laboratory ID = 20160560044 Lab Value = 0.018 Expected Conc. = 0.0604 Report level label = 0.04 Pct Recovery = 30% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl SpecificMix = 041415 Laboratory ID = 20160210080 Lab Value = 0.011 Expected Conc. = 0.0604 Report level label = 0.04 Pct Recovery = 18% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 041415 Laboratory ID = 20152950078 Lab Value = 0.020 Expected Conc. = 0.0604 Report level label = 0.04 Pct Recovery = 33% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 041415 Laboratory ID = 20152040177 Lab Value = 0.035 Expected Conc. = 0.0604 Report level label = 0.04 Pct Recovery = 58% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl SpecificMix = 041415 Laboratory ID = 20151210037 Lab Value = 0.036 Expected Conc. = 0.0604 Report level label = 0.04 Pct Recovery = 60% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 041415 Laboratory ID = 20133400002 Lab Value = 0.041 Expected Conc. = 0.0604 Report level label = 0.04 Pct Recovery = 68% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = 052412 Laboratory ID = 20132910008 Lab Value = 0.036 Expected Conc. = 0.0604 Report level label = 0.04 Pct Recovery = 60% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = 052412 Laboratory ID = 20130650005 Lab Value = 0.034 Expected Conc. = 0.0604 Report level label = 0.04 Pct Recovery = 56% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl SpecificMix = 052412 Laboratory ID = 20140860102 Lab Value = 0.036 Expected Conc. = 0.0602 Report level label = 0.04 Pct Recovery = 60% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 012513 Laboratory ID = 20131920149 Lab Value = 0.031 Expected Conc. = 0.0602 Report level label = 0.04 Pct Recovery = 51% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl SpecificMix = 012513 Laboratory ID = 20160070059 Lab Value = 0.015 Expected Conc. = 0.06 Report level label = 0.04 Pct Recovery = 25% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = EN150514012 Laboratory ID = 20153160001 Lab Value = 0.024 Expected Conc. = 0.06 Report level label = 0.04 Pct Recovery = 40% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = EN150514012 Laboratory ID = 20151760208 Lab Value = 0.025 Expected Conc. = 0.06 Report level label = 0.04 Pct Recovery = 42% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl SpecificMix = EN150514012 Laboratory ID = 20151480170 Lab Value = 0.038 Expected Conc. = 0.06 Report level label = 0.04 Pct Recovery = 63% Analysis Date = 06/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150514012 Laboratory ID = 20131230084 Lab Value = 0.061 Expected Conc. = 0.0598 Report level label = 0.04 Pct Recovery = 102% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl SpecificMix = 05BB029 Laboratory ID = 20130510051 Lab Value = 0.047 Expected Conc. = 0.0598 Report level label = 0.04 Pct Recovery = 79% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl SpecificMix = 05BB029 Analysis Date = 02/08/18 Pct Recovery = 60% Analysis Date = 01/29/18 Pct Recovery = 60% Analysis Date = 01/29/18 Pct Recovery = 60% Analysis Date = 01/20/18 Pct Recovery = 59% Analysis Date = 01/20/18 Pct Recovery = 59% Analysis Date = 01/11/18 Pct Recovery = 59% Analysis Date = 01/11/18 Pct Recovery = 59% Analysis Date = 01/02/18 Pct Recovery = 59% Analysis Date = 01/02/18 Pct Recovery = 59% Analysis Date = 12/23/17 Pct Recovery = 59% Analysis Date = 12/23/17 Pct Recovery = 59% Analysis Date = 12/14/17 Pct Recovery = 58% Analysis Date = 12/14/17 Pct Recovery = 58% Analysis Date = 12/05/17 Pct Recovery = 58% Analysis Date = 12/05/17 Pct Recovery = 58% Analysis Date = 11/26/17 Pct Recovery = 58% Analysis Date = 11/26/17 Pct Recovery = 58% Analysis Date = 11/16/17 Pct Recovery = 58% Analysis Date = 11/16/17 Pct Recovery = 58% Analysis Date = 11/07/17 Pct Recovery = 57% Analysis Date = 11/07/17 Pct Recovery = 57% Analysis Date = 10/29/17 Pct Recovery = 57% Analysis Date = 10/29/17 Pct Recovery = 57% Analysis Date = 10/20/17 Pct Recovery = 57% Analysis Date = 10/20/17 Pct Recovery = 57% Analysis Date = 10/10/17 Pct Recovery = 57% Analysis Date = 10/10/17 Pct Recovery = 57% Analysis Date = 10/01/17 Pct Recovery = 56% Analysis Date = 10/01/17 Pct Recovery = 56% Analysis Date = 09/22/17 Pct Recovery = 56% Analysis Date = 09/22/17 Pct Recovery = 56% Analysis Date = 09/13/17 Pct Recovery = 56% Analysis Date = 09/13/17 Pct Recovery = 56% Analysis Date = 09/03/17 Pct Recovery = 56% Analysis Date = 09/03/17 Pct Recovery = 56% Analysis Date = 08/25/17 Pct Recovery = 55% Analysis Date = 08/25/17 Pct Recovery = 55% Analysis Date = 08/16/17 Pct Recovery = 55% Analysis Date = 08/16/17 Pct Recovery = 55% Analysis Date = 08/07/17 Pct Recovery = 55% Analysis Date = 08/07/17 Pct Recovery = 55% Analysis Date = 07/28/17 Pct Recovery = 54% Analysis Date = 07/28/17 Pct Recovery = 54% Analysis Date = 07/19/17 Pct Recovery = 54% Analysis Date = 07/19/17 Pct Recovery = 54% Analysis Date = 07/10/17 Pct Recovery = 54% Analysis Date = 07/10/17 Pct Recovery = 54% Analysis Date = 07/01/17 Pct Recovery = 54% Analysis Date = 07/01/17 Pct Recovery = 54% Analysis Date = 06/22/17 Pct Recovery = 53% Analysis Date = 06/22/17 Pct Recovery = 53% Analysis Date = 06/12/17 Pct Recovery = 53% Analysis Date = 06/12/17 Pct Recovery = 53% Analysis Date = 06/03/17 Pct Recovery = 53% Analysis Date = 06/03/17 Pct Recovery = 53% Analysis Date = 05/25/17 Pct Recovery = 53% Analysis Date = 05/25/17 Pct Recovery = 53% Analysis Date = 05/16/17 Pct Recovery = 52% Analysis Date = 05/16/17 Pct Recovery = 52% Analysis Date = 05/06/17 Pct Recovery = 52% Analysis Date = 05/06/17 Pct Recovery = 52% Analysis Date = 04/27/17 Pct Recovery = 52% Analysis Date = 04/27/17 Pct Recovery = 52% Analysis Date = 04/18/17 Pct Recovery = 52% Analysis Date = 04/18/17 Pct Recovery = 52% Analysis Date = 04/09/17 Pct Recovery = 51% Analysis Date = 04/09/17 Pct Recovery = 51% Analysis Date = 03/30/17 Pct Recovery = 51% Analysis Date = 03/30/17 Pct Recovery = 51% Analysis Date = 03/21/17 Pct Recovery = 51% Analysis Date = 03/21/17 Pct Recovery = 51% Analysis Date = 03/12/17 Pct Recovery = 51% Analysis Date = 03/12/17 Pct Recovery = 51% Analysis Date = 03/03/17 Pct Recovery = 50% Analysis Date = 03/03/17 Pct Recovery = 50% Analysis Date = 02/21/17 Pct Recovery = 50% Analysis Date = 02/21/17 Pct Recovery = 50% Analysis Date = 02/12/17 Pct Recovery = 50% Analysis Date = 02/12/17 Pct Recovery = 50% Analysis Date = 02/03/17 Pct Recovery = 50% Analysis Date = 02/03/17 Pct Recovery = 50% Analysis Date = 01/25/17 Pct Recovery = 50% Analysis Date = 01/25/17 Pct Recovery = 50% Analysis Date = 01/15/17 Pct Recovery = 49% Analysis Date = 01/15/17 Pct Recovery = 49% Analysis Date = 01/06/17 Pct Recovery = 49% Analysis Date = 01/06/17 Pct Recovery = 49% Analysis Date = 12/28/16 Pct Recovery = 49% Analysis Date = 12/28/16 Pct Recovery = 49% Analysis Date = 12/19/16 Pct Recovery = 49% Analysis Date = 12/19/16 Pct Recovery = 49% Analysis Date = 12/09/16 Pct Recovery = 49% Analysis Date = 12/09/16 Pct Recovery = 49% Analysis Date = 11/30/16 Pct Recovery = 48% Analysis Date = 11/30/16 Pct Recovery = 48% Analysis Date = 11/21/16 Pct Recovery = 48% Analysis Date = 11/21/16 Pct Recovery = 48% Analysis Date = 11/12/16 Pct Recovery = 48% Analysis Date = 11/12/16 Pct Recovery = 48% Analysis Date = 11/03/16 Pct Recovery = 48% Analysis Date = 11/03/16 Pct Recovery = 48% Analysis Date = 10/24/16 Pct Recovery = 48% Analysis Date = 10/24/16 Pct Recovery = 48% Analysis Date = 10/15/16 Pct Recovery = 47% Analysis Date = 10/15/16 Pct Recovery = 47% Analysis Date = 10/06/16 Pct Recovery = 47% Analysis Date = 10/06/16 Pct Recovery = 47% Analysis Date = 09/27/16 Pct Recovery = 47% Analysis Date = 09/27/16 Pct Recovery = 47% Analysis Date = 09/17/16 Pct Recovery = 47% Analysis Date = 09/17/16 Pct Recovery = 47% Analysis Date = 09/08/16 Pct Recovery = 47% Analysis Date = 09/08/16 Pct Recovery = 47% Analysis Date = 08/30/16 Pct Recovery = 46% Analysis Date = 08/30/16 Pct Recovery = 46% Analysis Date = 08/21/16 Pct Recovery = 46% Analysis Date = 08/21/16 Pct Recovery = 46% Analysis Date = 08/11/16 Pct Recovery = 46% Analysis Date = 08/11/16 Pct Recovery = 46% Analysis Date = 08/02/16 Pct Recovery = 46% Analysis Date = 08/02/16 Pct Recovery = 46% Analysis Date = 07/24/16 Pct Recovery = 46% Analysis Date = 07/24/16 Pct Recovery = 46% Analysis Date = 07/15/16 Pct Recovery = 45% Analysis Date = 07/15/16 Pct Recovery = 45% Analysis Date = 07/05/16 Pct Recovery = 45% Analysis Date = 07/05/16 Pct Recovery = 45% Analysis Date = 06/26/16 Pct Recovery = 45% Analysis Date = 06/26/16 Pct Recovery = 45% Analysis Date = 06/17/16 Pct Recovery = 45% Analysis Date = 06/17/16 Pct Recovery = 45% Analysis Date = 06/08/16 Pct Recovery = 45% Analysis Date = 06/08/16 Pct Recovery = 45% Analysis Date = 05/29/16 Pct Recovery = 44% Analysis Date = 05/29/16 Pct Recovery = 44% Analysis Date = 05/20/16 Pct Recovery = 44% Analysis Date = 05/20/16 Pct Recovery = 44% Analysis Date = 05/11/16 Pct Recovery = 44% Analysis Date = 05/11/16 Pct Recovery = 44% Analysis Date = 05/02/16 Pct Recovery = 44% Analysis Date = 05/02/16 Pct Recovery = 44% Analysis Date = 04/22/16 Pct Recovery = 44% Analysis Date = 04/22/16 Pct Recovery = 44% Analysis Date = 04/13/16 Pct Recovery = 44% Analysis Date = 04/13/16 Pct Recovery = 44% Analysis Date = 04/04/16 Pct Recovery = 44% Analysis Date = 04/04/16 Pct Recovery = 44% Analysis Date = 03/26/16 Pct Recovery = 44% Analysis Date = 03/26/16 Pct Recovery = 44% Analysis Date = 03/17/16 Pct Recovery = 44% Analysis Date = 03/17/16 Pct Recovery = 44% Analysis Date = 03/07/16 Pct Recovery = 43% Analysis Date = 03/07/16 Pct Recovery = 43% Analysis Date = 02/27/16 Pct Recovery = 43% Analysis Date = 02/27/16 Pct Recovery = 43% Analysis Date = 02/18/16 Pct Recovery = 43% Analysis Date = 02/18/16 Pct Recovery = 43% Analysis Date = 02/09/16 Pct Recovery = 43% Analysis Date = 02/09/16 Pct Recovery = 43% Analysis Date = 01/30/16 Pct Recovery = 43% Analysis Date = 01/30/16 Pct Recovery = 43% Analysis Date = 01/21/16 Pct Recovery = 43% Analysis Date = 01/21/16 Pct Recovery = 43% Analysis Date = 01/12/16 Pct Recovery = 43% Analysis Date = 01/12/16 Pct Recovery = 43% Analysis Date = 01/03/16 Pct Recovery = 43% Analysis Date = 01/03/16 Pct Recovery = 43% Analysis Date = 12/24/15 Pct Recovery = 43% Analysis Date = 12/24/15 Pct Recovery = 43% Analysis Date = 12/15/15 Pct Recovery = 43% Analysis Date = 12/15/15 Pct Recovery = 43% Analysis Date = 12/06/15 Pct Recovery = 44% Analysis Date = 12/06/15 Pct Recovery = 44% Analysis Date = 11/27/15 Pct Recovery = 44% Analysis Date = 11/27/15 Pct Recovery = 44% Analysis Date = 11/17/15 Pct Recovery = 44% Analysis Date = 11/17/15 Pct Recovery = 44% Analysis Date = 11/08/15 Pct Recovery = 44% Analysis Date = 11/08/15 Pct Recovery = 44% Analysis Date = 10/30/15 Pct Recovery = 44% Analysis Date = 10/30/15 Pct Recovery = 44% Analysis Date = 10/21/15 Pct Recovery = 44% Analysis Date = 10/21/15 Pct Recovery = 44% Analysis Date = 10/11/15 Pct Recovery = 44% Analysis Date = 10/11/15 Pct Recovery = 44% Analysis Date = 10/02/15 Pct Recovery = 45% Analysis Date = 10/02/15 Pct Recovery = 45% Analysis Date = 09/23/15 Pct Recovery = 45% Analysis Date = 09/23/15 Pct Recovery = 45% Analysis Date = 09/14/15 Pct Recovery = 45% Analysis Date = 09/14/15 Pct Recovery = 45% Analysis Date = 09/04/15 Pct Recovery = 45% Analysis Date = 09/04/15 Pct Recovery = 45% Analysis Date = 08/26/15 Pct Recovery = 45% Analysis Date = 08/26/15 Pct Recovery = 45% Analysis Date = 08/17/15 Pct Recovery = 45% Analysis Date = 08/17/15 Pct Recovery = 45% Analysis Date = 08/08/15 Pct Recovery = 45% Analysis Date = 08/08/15 Pct Recovery = 45% Analysis Date = 07/30/15 Pct Recovery = 45% Analysis Date = 07/30/15 Pct Recovery = 45% Analysis Date = 07/20/15 Pct Recovery = 46% Analysis Date = 07/20/15 Pct Recovery = 46% Analysis Date = 07/11/15 Pct Recovery = 46% Analysis Date = 07/11/15 Pct Recovery = 46% Analysis Date = 07/02/15 Pct Recovery = 46% Analysis Date = 07/02/15 Pct Recovery = 46% Analysis Date = 06/23/15 Pct Recovery = 46% Analysis Date = 06/23/15 Pct Recovery = 46% Analysis Date = 06/13/15 Pct Recovery = 47% Analysis Date = 06/13/15 Pct Recovery = 47% Analysis Date = 06/04/15 Pct Recovery = 47% Analysis Date = 06/04/15 Pct Recovery = 47% Analysis Date = 05/26/15 Pct Recovery = 48% Analysis Date = 05/26/15 Pct Recovery = 48% Analysis Date = 05/17/15 Pct Recovery = 48% Analysis Date = 05/17/15 Pct Recovery = 48% Analysis Date = 05/07/15 Pct Recovery = 48% Analysis Date = 05/07/15 Pct Recovery = 48% Analysis Date = 04/28/15 Pct Recovery = 49% Analysis Date = 04/28/15 Pct Recovery = 49% Analysis Date = 04/19/15 Pct Recovery = 49% Analysis Date = 04/19/15 Pct Recovery = 49% Analysis Date = 04/10/15 Pct Recovery = 49% Analysis Date = 04/10/15 Pct Recovery = 49% Analysis Date = 03/31/15 Pct Recovery = 50% Analysis Date = 03/31/15 Pct Recovery = 50% Analysis Date = 03/22/15 Pct Recovery = 50% Analysis Date = 03/22/15 Pct Recovery = 50% Analysis Date = 03/13/15 Pct Recovery = 50% Analysis Date = 03/13/15 Pct Recovery = 50% Analysis Date = 03/04/15 Pct Recovery = 51% Analysis Date = 03/04/15 Pct Recovery = 51% Analysis Date = 02/22/15 Pct Recovery = 51% Analysis Date = 02/22/15 Pct Recovery = 51% Analysis Date = 02/13/15 Pct Recovery = 51% Analysis Date = 02/13/15 Pct Recovery = 51% Analysis Date = 02/04/15 Pct Recovery = 52% Analysis Date = 02/04/15 Pct Recovery = 52% Analysis Date = 01/26/15 Pct Recovery = 52% Analysis Date = 01/26/15 Pct Recovery = 52% Analysis Date = 01/16/15 Pct Recovery = 52% Analysis Date = 01/16/15 Pct Recovery = 52% Analysis Date = 01/07/15 Pct Recovery = 52% Analysis Date = 01/07/15 Pct Recovery = 52% Analysis Date = 12/29/14 Pct Recovery = 52% Analysis Date = 12/29/14 Pct Recovery = 52% Analysis Date = 12/20/14 Pct Recovery = 53% Analysis Date = 12/20/14 Pct Recovery = 53% Analysis Date = 12/11/14 Pct Recovery = 53% Analysis Date = 12/11/14 Pct Recovery = 53% Analysis Date = 12/01/14 Pct Recovery = 53% Analysis Date = 12/01/14 Pct Recovery = 53% Analysis Date = 11/22/14 Pct Recovery = 53% Analysis Date = 11/22/14 Pct Recovery = 53% Analysis Date = 11/13/14 Pct Recovery = 53% Analysis Date = 11/13/14 Pct Recovery = 53% Analysis Date = 11/04/14 Pct Recovery = 53% Analysis Date = 11/04/14 Pct Recovery = 53% Analysis Date = 10/25/14 Pct Recovery = 54% Analysis Date = 10/25/14 Pct Recovery = 54% Analysis Date = 10/16/14 Pct Recovery = 54% Analysis Date = 10/16/14 Pct Recovery = 54% Analysis Date = 10/07/14 Pct Recovery = 54% Analysis Date = 10/07/14 Pct Recovery = 54% Analysis Date = 09/28/14 Pct Recovery = 54% Analysis Date = 09/28/14 Pct Recovery = 54% Analysis Date = 09/18/14 Pct Recovery = 54% Analysis Date = 09/18/14 Pct Recovery = 54% Analysis Date = 09/09/14 Pct Recovery = 54% Analysis Date = 09/09/14 Pct Recovery = 54% Analysis Date = 08/31/14 Pct Recovery = 55% Analysis Date = 08/31/14 Pct Recovery = 55% Analysis Date = 08/22/14 Pct Recovery = 55% Analysis Date = 08/22/14 Pct Recovery = 55% Analysis Date = 08/12/14 Pct Recovery = 55% Analysis Date = 08/12/14 Pct Recovery = 55% Analysis Date = 08/03/14 Pct Recovery = 55% Analysis Date = 08/03/14 Pct Recovery = 55% Analysis Date = 07/25/14 Pct Recovery = 55% Analysis Date = 07/25/14 Pct Recovery = 55% Analysis Date = 07/16/14 Pct Recovery = 56% Analysis Date = 07/16/14 Pct Recovery = 56% Analysis Date = 07/06/14 Pct Recovery = 56% Analysis Date = 07/06/14 Pct Recovery = 56% Analysis Date = 06/27/14 Pct Recovery = 56% Analysis Date = 06/27/14 Pct Recovery = 56% Analysis Date = 06/18/14 Pct Recovery = 56% Analysis Date = 06/18/14 Pct Recovery = 56% Analysis Date = 06/09/14 Pct Recovery = 56% Analysis Date = 06/09/14 Pct Recovery = 56% Analysis Date = 05/30/14 Pct Recovery = 57% Analysis Date = 05/30/14 Pct Recovery = 57% Analysis Date = 05/21/14 Pct Recovery = 57% Analysis Date = 05/21/14 Pct Recovery = 57% Analysis Date = 05/12/14 Pct Recovery = 57% Analysis Date = 05/12/14 Pct Recovery = 57% Analysis Date = 05/03/14 Pct Recovery = 57% Analysis Date = 05/03/14 Pct Recovery = 57% Analysis Date = 04/24/14 Pct Recovery = 58% Analysis Date = 04/24/14 Pct Recovery = 58% Analysis Date = 04/14/14 Pct Recovery = 58% Analysis Date = 04/14/14 Pct Recovery = 58% Analysis Date = 04/05/14 Pct Recovery = 58% Analysis Date = 04/05/14 Pct Recovery = 58% Analysis Date = 03/27/14 Pct Recovery = 59% Analysis Date = 03/27/14 Pct Recovery = 59% Analysis Date = 03/18/14 Pct Recovery = 59% Analysis Date = 03/18/14 Pct Recovery = 59% Analysis Date = 03/08/14 Pct Recovery = 59% Analysis Date = 03/08/14 Pct Recovery = 59% Analysis Date = 02/27/14 Pct Recovery = 59% Analysis Date = 02/27/14 Pct Recovery = 59% Analysis Date = 02/18/14 Pct Recovery = 60% Analysis Date = 02/18/14 Pct Recovery = 60% Analysis Date = 02/09/14 Pct Recovery = 60% Analysis Date = 02/09/14 Pct Recovery = 60% Analysis Date = 01/30/14 Pct Recovery = 60% Analysis Date = 01/30/14 Pct Recovery = 60% Analysis Date = 01/21/14 Pct Recovery = 61% Analysis Date = 01/21/14 Pct Recovery = 61% Analysis Date = 01/12/14 Pct Recovery = 61% Analysis Date = 01/12/14 Pct Recovery = 61% Analysis Date = 01/03/14 Pct Recovery = 61% Analysis Date = 01/03/14 Pct Recovery = 61% Analysis Date = 12/24/13 Pct Recovery = 61% Analysis Date = 12/24/13 Pct Recovery = 61% Analysis Date = 12/15/13 Pct Recovery = 62% Analysis Date = 12/15/13 Pct Recovery = 62% Analysis Date = 12/06/13 Pct Recovery = 62% Analysis Date = 12/06/13 Pct Recovery = 62% Analysis Date = 11/27/13 Pct Recovery = 62% Analysis Date = 11/27/13 Pct Recovery = 62% Analysis Date = 11/17/13 Pct Recovery = 62% Analysis Date = 11/17/13 Pct Recovery = 62% Analysis Date = 11/08/13 Pct Recovery = 63% Analysis Date = 11/08/13 Pct Recovery = 63% Analysis Date = 10/30/13 Pct Recovery = 63% Analysis Date = 10/30/13 Pct Recovery = 63% Analysis Date = 10/21/13 Pct Recovery = 63% Analysis Date = 10/21/13 Pct Recovery = 63% Analysis Date = 10/11/13 Pct Recovery = 63% Analysis Date = 10/11/13 Pct Recovery = 63% Analysis Date = 10/02/13 Pct Recovery = 64% Analysis Date = 10/02/13 Pct Recovery = 64% Analysis Date = 09/23/13 Pct Recovery = 64% Analysis Date = 09/23/13 Pct Recovery = 64% Analysis Date = 09/14/13 Pct Recovery = 64% Analysis Date = 09/14/13 Pct Recovery = 64% Analysis Date = 09/05/13 Pct Recovery = 64% Analysis Date = 09/05/13 Pct Recovery = 64% Analysis Date = 08/26/13 Pct Recovery = 64% Analysis Date = 08/26/13 Pct Recovery = 64% Analysis Date = 08/17/13 Pct Recovery = 65% Analysis Date = 08/17/13 Pct Recovery = 65% Analysis Date = 08/08/13 Pct Recovery = 65% Analysis Date = 08/08/13 Pct Recovery = 65% Analysis Date = 07/30/13 Pct Recovery = 65% Analysis Date = 07/30/13 Pct Recovery = 65% Analysis Date = 07/20/13 Pct Recovery = 65% Analysis Date = 07/20/13 Pct Recovery = 65% Analysis Date = 07/11/13 Pct Recovery = 66% Analysis Date = 07/11/13 Pct Recovery = 66% Analysis Date = 07/02/13 Pct Recovery = 66% Analysis Date = 07/02/13 Pct Recovery = 66% Analysis Date = 06/23/13 Pct Recovery = 66% Analysis Date = 06/23/13 Pct Recovery = 66% Analysis Date = 06/13/13 Pct Recovery = 66% Analysis Date = 06/13/13 Pct Recovery = 66% Analysis Date = 06/04/13 Pct Recovery = 67% Analysis Date = 06/04/13 Pct Recovery = 67% Analysis Date = 05/26/13 Pct Recovery = 67% Analysis Date = 05/26/13 Pct Recovery = 67% Analysis Date = 05/17/13 Pct Recovery = 67% Analysis Date = 05/17/13 Pct Recovery = 67% Analysis Date = 05/07/13 Pct Recovery = 67% Analysis Date = 05/07/13 Pct Recovery = 67% Analysis Date = 04/28/13 Pct Recovery = 68% Analysis Date = 04/28/13 Pct Recovery = 68% Analysis Date = 04/19/13 Pct Recovery = 68% Analysis Date = 04/19/13 Pct Recovery = 68% Analysis Date = 04/10/13 Pct Recovery = 68% Analysis Date = 04/10/13 Pct Recovery = 68% Analysis Date = 03/31/13 Pct Recovery = 68% Analysis Date = 03/31/13 Pct Recovery = 68% Analysis Date = 03/22/13 Pct Recovery = 68% Analysis Date = 03/22/13 Pct Recovery = 68% Analysis Date = 03/13/13 Pct Recovery = 69% Analysis Date = 03/13/13 Pct Recovery = 69% Analysis Date = 03/04/13 Pct Recovery = 69% Analysis Date = 03/04/13 Pct Recovery = 69% Analysis Date = 02/22/13 Pct Recovery = 69% Analysis Date = 02/22/13 Pct Recovery = 69% Analysis Date = 02/13/13 Pct Recovery = 69% Analysis Date = 02/13/13 Pct Recovery = 69% Analysis Date = 02/04/13 Pct Recovery = 70% Analysis Date = 02/04/13 Pct Recovery = 70% Analysis Date = 01/26/13 Pct Recovery = 70% Analysis Date = 01/26/13 Pct Recovery = 70% Analysis Date = 01/17/13 Pct Recovery = 70% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
DICHLOROVOS (DICHLORVOS)

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 75 54% 20% 51% 19%
Total 75 54% 20% 51% 19%

Sample Statistics
DICHLOROVOS (DICHLORVOS)

Characteristic N % % Basis
Plotted 75 100% Spiked
Estimated Values 75 100% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 75 .  
False Negatives 0 0% 0 out of 75
Not Spiked 43 .  
False Positives 0 0% 0 out of 43

OBSP Determination:
DICROTOPHOS
METHOD: 2033 , TESTIDCODE: 38454GCM39

Laboratory ID = 20140100085 Lab Value = 0.225 Expected Conc. = 1.009 Report level label = 0.08 Pct Recovery = 22% Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl SpecificMix = 042413 Laboratory ID = 20180390003 Lab Value = 0.081 Expected Conc. = 0.531 Report level label = 0.14 Pct Recovery = 15% Analysis Date = 04/06/18 SpikeMix = Spex Organics EN170808006: 100 µl & Abs 071717Pest: 100 µl SpecificMix = EN170808006 Laboratory ID = 20132690010 Lab Value = 0.154 Expected Conc. = 0.5045 Report level label = 0.08 Pct Recovery = 31% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl SpecificMix = 042413 Laboratory ID = 20132560001 Lab Value = 0.123 Expected Conc. = 0.5045 Report level label = 0.08 Pct Recovery = 24% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl SpecificMix = 042413 Laboratory ID = 20163370001 Lab Value = 0.103 Expected Conc. = 0.502 Report level label = 0.08 Pct Recovery = 21% Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl SpecificMix = B20160331 Laboratory ID = 20163150006 Lab Value = 0.103 Expected Conc. = 0.502 Report level label = 0.08 Pct Recovery = 21% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl SpecificMix = B20160331 Laboratory ID = 20161880109 Lab Value = 0.093 Expected Conc. = 0.502 Report level label = 0.08 Pct Recovery = 19% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl SpecificMix = 03FF076 Laboratory ID = 20130250061 Lab Value = 0.075 Expected Conc. = 0.498 Report level label = 0.08 Pct Recovery = 15% Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl SpecificMix = 05BB029 Laboratory ID = 20132140002 Lab Value = 0.088 Expected Conc. = 0.4975 Report level label = 0.08 Pct Recovery = 18% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl SpecificMix = 04CC101 Laboratory ID = 20152460215 Lab Value = 0.119 Expected Conc. = 0.4792 Report level label = 0.08 Pct Recovery = 25% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl SpecificMix = 0406-15-01 Laboratory ID = 20171720140 Lab Value = 0.099 Expected Conc. = 0.4016 Report level label = 0.08 Pct Recovery = 25% Analysis Date = 08/31/17 SpikeMix = Supelco LC20138V: 80 µl & Phenova B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20171660002 Lab Value = 0.110 Expected Conc. = 0.4016 Report level label = 0.08 Pct Recovery = 27% Analysis Date = 08/23/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20170960001 Lab Value = 0.068 Expected Conc. = 0.4016 Report level label = 0.08 Pct Recovery = 17% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl SpecificMix = 03FF076 Laboratory ID = 20170190026 Lab Value = 0.066 Expected Conc. = 0.4016 Report level label = 0.08 Pct Recovery = 16% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20161470001 Lab Value = 0.086 Expected Conc. = 0.4016 Report level label = 0.08 Pct Recovery = 21% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20150720069 Lab Value = 0.005 Expected Conc. = 0.3216 Report level label = 0.08 Pct Recovery = 2% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 0227-14-08 Laboratory ID = 20141770149 Lab Value = 0.064 Expected Conc. = 0.3216 Report level label = 0.08 Pct Recovery = 20% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl SpecificMix = 0227-14-08 Laboratory ID = 20141570088 Lab Value = 0.094 Expected Conc. = 0.3216 Report level label = 0.08 Pct Recovery = 29% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl SpecificMix = 0227-14-08 Laboratory ID = 20143240095 Lab Value = 0.098 Expected Conc. = 0.3192 Report level label = 0.08 Pct Recovery = 31% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl SpecificMix = 042814 Laboratory ID = 20142960086 Lab Value = 0.072 Expected Conc. = 0.3192 Report level label = 0.08 Pct Recovery = 23% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 042814 Laboratory ID = 20142530087 Lab Value = 0.067 Expected Conc. = 0.3192 Report level label = 0.08 Pct Recovery = 21% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl SpecificMix = 042814 Laboratory ID = 20172230001 Lab Value = 0.087 Expected Conc. = 0.27 Report level label = 0.08 Pct Recovery = 32% Analysis Date = 10/19/17 SpikeMix = ChemService 6472100: 50 µl & Abs 071717Pest: 50 µl SpecificMix = 6472100 Laboratory ID = 20181430122 Lab Value = 0.070 Expected Conc. = 0.2655 Report level label = 0.14 Pct Recovery = 26% Analysis Date = 06/20/18 SpikeMix = Abs 071817Pest: 50 µl & Spex Organics EN170808006: 50 µl SpecificMix = EN170808006 Laboratory ID = 20172560101 Lab Value = 0.052 Expected Conc. = 0.2655 Report level label = 0.08 Pct Recovery = 20% Analysis Date = 12/22/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6567600: 50 µl SpecificMix = EN170808006 Laboratory ID = 20172370001 Lab Value = 0.062 Expected Conc. = 0.2655 Report level label = 0.08 Pct Recovery = 23% Analysis Date = 11/18/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6537100: 50 µl SpecificMix = EN170808006 Laboratory ID = 20130940097 Lab Value = 0.066 Expected Conc. = 0.2525 Report level label = 0.08 Pct Recovery = 26% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = 052412 Laboratory ID = 20130100066 Lab Value = 0.072 Expected Conc. = 0.2525 Report level label = 0.08 Pct Recovery = 29% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl SpecificMix = 052412 Laboratory ID = 20140230082 Lab Value = 0.059 Expected Conc. = 0.2505 Report level label = 0.08 Pct Recovery = 24% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl SpecificMix = 012513 Laboratory ID = 20132420001 Lab Value = 0.060 Expected Conc. = 0.2505 Report level label = 0.08 Pct Recovery = 24% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl SpecificMix = 012513 Laboratory ID = 20160770090 Lab Value = 0.033 Expected Conc. = 0.2396 Report level label = 0.08 Pct Recovery = 14% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20160630046 Lab Value = 0.032 Expected Conc. = 0.2396 Report level label = 0.08 Pct Recovery = 13% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20153510109 Lab Value = 0.025 Expected Conc. = 0.2396 Report level label = 0.08 Pct Recovery = 10% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20153440001 Lab Value = 0.022 Expected Conc. = 0.2396 Report level label = 0.08 Pct Recovery = 9% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20133580036 Lab Value = 0.038 Expected Conc. = 0.2018 Report level label = 0.08 Pct Recovery = 19% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 042413 Laboratory ID = 20133190012 Lab Value = 0.070 Expected Conc. = 0.2018 Report level label = 0.08 Pct Recovery = 35% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 042413 Laboratory ID = 20131650073 Lab Value = 0.080 Expected Conc. = 0.2018 Report level label = 0.08 Pct Recovery = 40% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl SpecificMix = 042413 Laboratory ID = 20172020035 Lab Value = 0.049 Expected Conc. = 0.2008 Report level label = 0.08 Pct Recovery = 24% Analysis Date = 11/07/17 SpikeMix = Abs 071717Pest: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20171510080 Lab Value = 0.045 Expected Conc. = 0.2008 Report level label = 0.08 Pct Recovery = 22% Analysis Date = 06/09/17 SpikeMix = Supelco LC20138V: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20171160110 Lab Value = 0.050 Expected Conc. = 0.2008 Report level label = 0.08 Pct Recovery = 25% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = B20160331 Laboratory ID = 20170460061 Lab Value = 0.034 Expected Conc. = 0.2008 Report level label = 0.08 Pct Recovery = 17% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl SpecificMix = 03FF076 Laboratory ID = 20162660005 Lab Value = 0.035 Expected Conc. = 0.2008 Report level label = 0.08 Pct Recovery = 17% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl SpecificMix = 03FF076 Laboratory ID = 20162380004 Lab Value = 0.049 Expected Conc. = 0.2008 Report level label = 0.08 Pct Recovery = 24% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = B20160331 Laboratory ID = 20162150213 Lab Value = 0.029 Expected Conc. = 0.2008 Report level label = 0.08 Pct Recovery = 14% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl SpecificMix = B20160331 Laboratory ID = 20161600087 Lab Value = 0.025 Expected Conc. = 0.2008 Report level label = 0.08 Pct Recovery = 12% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20161340228 Lab Value = 0.023 Expected Conc. = 0.2008 Report level label = 0.08 Pct Recovery = 11% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl SpecificMix = 03FF076 Laboratory ID = 20161190075 Lab Value = 0.021 Expected Conc. = 0.2008 Report level label = 0.08 Pct Recovery = 10% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20140510043 Lab Value = 0.098 Expected Conc. = 0.199 Report level label = 0.08 Pct Recovery = 49% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 04CC101 Laboratory ID = 20133310030 Lab Value = 0.059 Expected Conc. = 0.199 Report level label = 0.08 Pct Recovery = 30% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl SpecificMix = 04CC101 Laboratory ID = 20132280016 Lab Value = 0.046 Expected Conc. = 0.199 Report level label = 0.08 Pct Recovery = 23% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl SpecificMix = 04CC101 Laboratory ID = 20131510026 Lab Value = 0.042 Expected Conc. = 0.199 Report level label = 0.08 Pct Recovery = 21% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl SpecificMix = 04CC101 Laboratory ID = 20180940080 Lab Value = 0.020 Expected Conc. = 0.162 Report level label = 0.14 Pct Recovery = 12% Analysis Date = 05/31/18 SpikeMix = ChemService 6472100: 30 µl & Abs 071717Pest: 30 µl SpecificMix = 6472100 Laboratory ID = 20180050004 Lab Value = 0.046 Expected Conc. = 0.162 Report level label = 0.14 Pct Recovery = 28% Analysis Date = 04/05/18 SpikeMix = Abs 071817Pest: 30 µl & ChemService 6472100: 30 µl SpecificMix = 6472100 Laboratory ID = 20173120093 Lab Value = 0.048 Expected Conc. = 0.162 Report level label = 0.08 Pct Recovery = 30% Analysis Date = 03/10/18 SpikeMix = ChemService 6472100: 30 µl & ChemService 6537100: 30 µl SpecificMix = 6472100 Laboratory ID = 20141840097 Lab Value = 0.034 Expected Conc. = 0.1608 Report level label = 0.08 Pct Recovery = 21% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20141490205 Lab Value = 0.051 Expected Conc. = 0.1608 Report level label = 0.08 Pct Recovery = 32% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20141420140 Lab Value = 0.042 Expected Conc. = 0.1608 Report level label = 0.08 Pct Recovery = 26% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20141360094 Lab Value = 0.033 Expected Conc. = 0.1608 Report level label = 0.08 Pct Recovery = 21% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20143370094 Lab Value = 0.042 Expected Conc. = 0.1596 Report level label = 0.08 Pct Recovery = 26% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl SpecificMix = 042814 Laboratory ID = 20142820151 Lab Value = 0.048 Expected Conc. = 0.1596 Report level label = 0.08 Pct Recovery = 30% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl SpecificMix = 042814 Laboratory ID = 20142470041 Lab Value = 0.048 Expected Conc. = 0.1596 Report level label = 0.08 Pct Recovery = 30% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl SpecificMix = 042814 Laboratory ID = 20142200164 Lab Value = 0.044 Expected Conc. = 0.1596 Report level label = 0.08 Pct Recovery = 28% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 042814 Laboratory ID = 20152190003 Lab Value = 0.040 Expected Conc. = 0.1198 Report level label = 0.08 Pct Recovery = 33% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = 0406-15-01 Laboratory ID = 20152040177 Lab Value = 0.053 Expected Conc. = 0.1198 Report level label = 0.08 Pct Recovery = 44% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl SpecificMix = 0406-15-01 Laboratory ID = 20133400002 Lab Value = 0.030 Expected Conc. = 0.101 Report level label = 0.08 Pct Recovery = 30% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = 052412 Laboratory ID = 20132910008 Lab Value = 0.026 Expected Conc. = 0.101 Report level label = 0.08 Pct Recovery = 26% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = 052412 Laboratory ID = 20130650005 Lab Value = 0.025 Expected Conc. = 0.101 Report level label = 0.08 Pct Recovery = 25% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl SpecificMix = 052412 Laboratory ID = 20140860102 Lab Value = 0.027 Expected Conc. = 0.1002 Report level label = 0.08 Pct Recovery = 27% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 012513 Laboratory ID = 20131920149 Lab Value = 0.023 Expected Conc. = 0.1002 Report level label = 0.08 Pct Recovery = 23% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl SpecificMix = 012513 Laboratory ID = 20131230084 Lab Value = 0.020 Expected Conc. = 0.0996 Report level label = 0.08 Pct Recovery = 20% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl SpecificMix = 05BB029 Laboratory ID = 20130510051 Lab Value = 0.019 Expected Conc. = 0.0996 Report level label = 0.08 Pct Recovery = 19% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl SpecificMix = 05BB029 Analysis Date = 06/20/18 Pct Recovery = 24% Analysis Date = 06/10/18 Pct Recovery = 24% Analysis Date = 06/10/18 Pct Recovery = 24% Analysis Date = 05/31/18 Pct Recovery = 24% Analysis Date = 05/31/18 Pct Recovery = 24% Analysis Date = 05/21/18 Pct Recovery = 24% Analysis Date = 05/21/18 Pct Recovery = 24% Analysis Date = 05/11/18 Pct Recovery = 24% Analysis Date = 05/11/18 Pct Recovery = 24% Analysis Date = 05/01/18 Pct Recovery = 24% Analysis Date = 05/01/18 Pct Recovery = 24% Analysis Date = 04/21/18 Pct Recovery = 24% Analysis Date = 04/21/18 Pct Recovery = 24% Analysis Date = 04/11/18 Pct Recovery = 23% Analysis Date = 04/11/18 Pct Recovery = 23% Analysis Date = 04/01/18 Pct Recovery = 23% Analysis Date = 04/01/18 Pct Recovery = 23% Analysis Date = 03/22/18 Pct Recovery = 23% Analysis Date = 03/22/18 Pct Recovery = 23% Analysis Date = 03/13/18 Pct Recovery = 23% Analysis Date = 03/13/18 Pct Recovery = 23% Analysis Date = 03/03/18 Pct Recovery = 23% Analysis Date = 03/03/18 Pct Recovery = 23% Analysis Date = 02/21/18 Pct Recovery = 23% Analysis Date = 02/21/18 Pct Recovery = 23% Analysis Date = 02/11/18 Pct Recovery = 23% Analysis Date = 02/11/18 Pct Recovery = 23% Analysis Date = 02/01/18 Pct Recovery = 23% Analysis Date = 02/01/18 Pct Recovery = 23% Analysis Date = 01/22/18 Pct Recovery = 23% Analysis Date = 01/22/18 Pct Recovery = 23% Analysis Date = 01/12/18 Pct Recovery = 23% Analysis Date = 01/12/18 Pct Recovery = 23% Analysis Date = 01/02/18 Pct Recovery = 23% Analysis Date = 01/02/18 Pct Recovery = 23% Analysis Date = 12/23/17 Pct Recovery = 23% Analysis Date = 12/23/17 Pct Recovery = 23% Analysis Date = 12/13/17 Pct Recovery = 22% Analysis Date = 12/13/17 Pct Recovery = 22% Analysis Date = 12/04/17 Pct Recovery = 22% Analysis Date = 12/04/17 Pct Recovery = 22% Analysis Date = 11/24/17 Pct Recovery = 22% Analysis Date = 11/24/17 Pct Recovery = 22% Analysis Date = 11/14/17 Pct Recovery = 22% Analysis Date = 11/14/17 Pct Recovery = 22% Analysis Date = 11/04/17 Pct Recovery = 22% Analysis Date = 11/04/17 Pct Recovery = 22% Analysis Date = 10/25/17 Pct Recovery = 22% Analysis Date = 10/25/17 Pct Recovery = 22% Analysis Date = 10/15/17 Pct Recovery = 22% Analysis Date = 10/15/17 Pct Recovery = 22% Analysis Date = 10/05/17 Pct Recovery = 22% Analysis Date = 10/05/17 Pct Recovery = 22% Analysis Date = 09/25/17 Pct Recovery = 22% Analysis Date = 09/25/17 Pct Recovery = 22% Analysis Date = 09/15/17 Pct Recovery = 22% Analysis Date = 09/15/17 Pct Recovery = 22% Analysis Date = 09/05/17 Pct Recovery = 22% Analysis Date = 09/05/17 Pct Recovery = 22% Analysis Date = 08/27/17 Pct Recovery = 21% Analysis Date = 08/27/17 Pct Recovery = 21% Analysis Date = 08/17/17 Pct Recovery = 21% Analysis Date = 08/17/17 Pct Recovery = 21% Analysis Date = 08/07/17 Pct Recovery = 21% Analysis Date = 08/07/17 Pct Recovery = 21% Analysis Date = 07/28/17 Pct Recovery = 21% Analysis Date = 07/28/17 Pct Recovery = 21% Analysis Date = 07/18/17 Pct Recovery = 21% Analysis Date = 07/18/17 Pct Recovery = 21% Analysis Date = 07/08/17 Pct Recovery = 21% Analysis Date = 07/08/17 Pct Recovery = 21% Analysis Date = 06/28/17 Pct Recovery = 21% Analysis Date = 06/28/17 Pct Recovery = 21% Analysis Date = 06/18/17 Pct Recovery = 21% Analysis Date = 06/18/17 Pct Recovery = 21% Analysis Date = 06/08/17 Pct Recovery = 21% Analysis Date = 06/08/17 Pct Recovery = 21% Analysis Date = 05/29/17 Pct Recovery = 21% Analysis Date = 05/29/17 Pct Recovery = 21% Analysis Date = 05/20/17 Pct Recovery = 21% Analysis Date = 05/20/17 Pct Recovery = 21% Analysis Date = 05/10/17 Pct Recovery = 21% Analysis Date = 05/10/17 Pct Recovery = 21% Analysis Date = 04/30/17 Pct Recovery = 21% Analysis Date = 04/30/17 Pct Recovery = 21% Analysis Date = 04/20/17 Pct Recovery = 21% Analysis Date = 04/20/17 Pct Recovery = 21% Analysis Date = 04/10/17 Pct Recovery = 20% Analysis Date = 04/10/17 Pct Recovery = 20% Analysis Date = 03/31/17 Pct Recovery = 20% Analysis Date = 03/31/17 Pct Recovery = 20% Analysis Date = 03/21/17 Pct Recovery = 20% Analysis Date = 03/21/17 Pct Recovery = 20% Analysis Date = 03/11/17 Pct Recovery = 20% Analysis Date = 03/11/17 Pct Recovery = 20% Analysis Date = 03/01/17 Pct Recovery = 20% Analysis Date = 03/01/17 Pct Recovery = 20% Analysis Date = 02/19/17 Pct Recovery = 20% Analysis Date = 02/19/17 Pct Recovery = 20% Analysis Date = 02/10/17 Pct Recovery = 20% Analysis Date = 02/10/17 Pct Recovery = 20% Analysis Date = 01/31/17 Pct Recovery = 20% Analysis Date = 01/31/17 Pct Recovery = 20% Analysis Date = 01/21/17 Pct Recovery = 20% Analysis Date = 01/21/17 Pct Recovery = 20% Analysis Date = 01/11/17 Pct Recovery = 20% Analysis Date = 01/11/17 Pct Recovery = 20% Analysis Date = 01/01/17 Pct Recovery = 20% Analysis Date = 01/01/17 Pct Recovery = 20% Analysis Date = 12/22/16 Pct Recovery = 20% Analysis Date = 12/22/16 Pct Recovery = 20% Analysis Date = 12/12/16 Pct Recovery = 20% Analysis Date = 12/12/16 Pct Recovery = 20% Analysis Date = 12/02/16 Pct Recovery = 20% Analysis Date = 12/02/16 Pct Recovery = 20% Analysis Date = 11/22/16 Pct Recovery = 20% Analysis Date = 11/22/16 Pct Recovery = 20% Analysis Date = 11/12/16 Pct Recovery = 20% Analysis Date = 11/12/16 Pct Recovery = 20% Analysis Date = 11/03/16 Pct Recovery = 19% Analysis Date = 11/03/16 Pct Recovery = 19% Analysis Date = 10/24/16 Pct Recovery = 19% Analysis Date = 10/24/16 Pct Recovery = 19% Analysis Date = 10/14/16 Pct Recovery = 19% Analysis Date = 10/14/16 Pct Recovery = 19% Analysis Date = 10/04/16 Pct Recovery = 19% Analysis Date = 10/04/16 Pct Recovery = 19% Analysis Date = 09/24/16 Pct Recovery = 19% Analysis Date = 09/24/16 Pct Recovery = 19% Analysis Date = 09/14/16 Pct Recovery = 19% Analysis Date = 09/14/16 Pct Recovery = 19% Analysis Date = 09/04/16 Pct Recovery = 19% Analysis Date = 09/04/16 Pct Recovery = 19% Analysis Date = 08/25/16 Pct Recovery = 19% Analysis Date = 08/25/16 Pct Recovery = 19% Analysis Date = 08/15/16 Pct Recovery = 19% Analysis Date = 08/15/16 Pct Recovery = 19% Analysis Date = 08/05/16 Pct Recovery = 19% Analysis Date = 08/05/16 Pct Recovery = 19% Analysis Date = 07/27/16 Pct Recovery = 19% Analysis Date = 07/27/16 Pct Recovery = 19% Analysis Date = 07/17/16 Pct Recovery = 19% Analysis Date = 07/17/16 Pct Recovery = 19% Analysis Date = 07/07/16 Pct Recovery = 19% Analysis Date = 07/07/16 Pct Recovery = 19% Analysis Date = 06/27/16 Pct Recovery = 19% Analysis Date = 06/27/16 Pct Recovery = 19% Analysis Date = 06/17/16 Pct Recovery = 19% Analysis Date = 06/17/16 Pct Recovery = 19% Analysis Date = 06/07/16 Pct Recovery = 19% Analysis Date = 06/07/16 Pct Recovery = 19% Analysis Date = 05/28/16 Pct Recovery = 19% Analysis Date = 05/28/16 Pct Recovery = 19% Analysis Date = 05/18/16 Pct Recovery = 19% Analysis Date = 05/18/16 Pct Recovery = 19% Analysis Date = 05/08/16 Pct Recovery = 19% Analysis Date = 05/08/16 Pct Recovery = 19% Analysis Date = 04/28/16 Pct Recovery = 19% Analysis Date = 04/28/16 Pct Recovery = 19% Analysis Date = 04/19/16 Pct Recovery = 19% Analysis Date = 04/19/16 Pct Recovery = 19% Analysis Date = 04/09/16 Pct Recovery = 19% Analysis Date = 04/09/16 Pct Recovery = 19% Analysis Date = 03/30/16 Pct Recovery = 19% Analysis Date = 03/30/16 Pct Recovery = 19% Analysis Date = 03/20/16 Pct Recovery = 19% Analysis Date = 03/20/16 Pct Recovery = 19% Analysis Date = 03/10/16 Pct Recovery = 19% Analysis Date = 03/10/16 Pct Recovery = 19% Analysis Date = 02/29/16 Pct Recovery = 19% Analysis Date = 02/29/16 Pct Recovery = 19% Analysis Date = 02/19/16 Pct Recovery = 19% Analysis Date = 02/19/16 Pct Recovery = 19% Analysis Date = 02/09/16 Pct Recovery = 19% Analysis Date = 02/09/16 Pct Recovery = 19% Analysis Date = 01/30/16 Pct Recovery = 20% Analysis Date = 01/30/16 Pct Recovery = 20% Analysis Date = 01/20/16 Pct Recovery = 20% Analysis Date = 01/20/16 Pct Recovery = 20% Analysis Date = 01/11/16 Pct Recovery = 20% Analysis Date = 01/11/16 Pct Recovery = 20% Analysis Date = 01/01/16 Pct Recovery = 20% Analysis Date = 01/01/16 Pct Recovery = 20% Analysis Date = 12/22/15 Pct Recovery = 20% Analysis Date = 12/22/15 Pct Recovery = 20% Analysis Date = 12/12/15 Pct Recovery = 20% Analysis Date = 12/12/15 Pct Recovery = 20% Analysis Date = 12/02/15 Pct Recovery = 20% Analysis Date = 12/02/15 Pct Recovery = 20% Analysis Date = 11/22/15 Pct Recovery = 20% Analysis Date = 11/22/15 Pct Recovery = 20% Analysis Date = 11/12/15 Pct Recovery = 20% Analysis Date = 11/12/15 Pct Recovery = 20% Analysis Date = 11/02/15 Pct Recovery = 20% Analysis Date = 11/02/15 Pct Recovery = 20% Analysis Date = 10/23/15 Pct Recovery = 20% Analysis Date = 10/23/15 Pct Recovery = 20% Analysis Date = 10/13/15 Pct Recovery = 20% Analysis Date = 10/13/15 Pct Recovery = 20% Analysis Date = 10/04/15 Pct Recovery = 20% Analysis Date = 10/04/15 Pct Recovery = 20% Analysis Date = 09/24/15 Pct Recovery = 20% Analysis Date = 09/24/15 Pct Recovery = 20% Analysis Date = 09/14/15 Pct Recovery = 20% Analysis Date = 09/14/15 Pct Recovery = 20% Analysis Date = 09/04/15 Pct Recovery = 21% Analysis Date = 09/04/15 Pct Recovery = 21% Analysis Date = 08/25/15 Pct Recovery = 21% Analysis Date = 08/25/15 Pct Recovery = 21% Analysis Date = 08/15/15 Pct Recovery = 21% Analysis Date = 08/15/15 Pct Recovery = 21% Analysis Date = 08/05/15 Pct Recovery = 21% Analysis Date = 08/05/15 Pct Recovery = 21% Analysis Date = 07/26/15 Pct Recovery = 21% Analysis Date = 07/26/15 Pct Recovery = 21% Analysis Date = 07/16/15 Pct Recovery = 22% Analysis Date = 07/16/15 Pct Recovery = 22% Analysis Date = 07/06/15 Pct Recovery = 22% Analysis Date = 07/06/15 Pct Recovery = 22% Analysis Date = 06/27/15 Pct Recovery = 22% Analysis Date = 06/27/15 Pct Recovery = 22% Analysis Date = 06/17/15 Pct Recovery = 22% Analysis Date = 06/17/15 Pct Recovery = 22% Analysis Date = 06/07/15 Pct Recovery = 22% Analysis Date = 06/07/15 Pct Recovery = 22% Analysis Date = 05/28/15 Pct Recovery = 22% Analysis Date = 05/28/15 Pct Recovery = 22% Analysis Date = 05/18/15 Pct Recovery = 23% Analysis Date = 05/18/15 Pct Recovery = 23% Analysis Date = 05/08/15 Pct Recovery = 23% Analysis Date = 05/08/15 Pct Recovery = 23% Analysis Date = 04/28/15 Pct Recovery = 23% Analysis Date = 04/28/15 Pct Recovery = 23% Analysis Date = 04/18/15 Pct Recovery = 23% Analysis Date = 04/18/15 Pct Recovery = 23% Analysis Date = 04/08/15 Pct Recovery = 23% Analysis Date = 04/08/15 Pct Recovery = 23% Analysis Date = 03/29/15 Pct Recovery = 23% Analysis Date = 03/29/15 Pct Recovery = 23% Analysis Date = 03/20/15 Pct Recovery = 24% Analysis Date = 03/20/15 Pct Recovery = 24% Analysis Date = 03/10/15 Pct Recovery = 24% Analysis Date = 03/10/15 Pct Recovery = 24% Analysis Date = 02/28/15 Pct Recovery = 24% Analysis Date = 02/28/15 Pct Recovery = 24% Analysis Date = 02/18/15 Pct Recovery = 24% Analysis Date = 02/18/15 Pct Recovery = 24% Analysis Date = 02/08/15 Pct Recovery = 24% Analysis Date = 02/08/15 Pct Recovery = 24% Analysis Date = 01/29/15 Pct Recovery = 24% Analysis Date = 01/29/15 Pct Recovery = 24% Analysis Date = 01/19/15 Pct Recovery = 25% Analysis Date = 01/19/15 Pct Recovery = 25% Analysis Date = 01/09/15 Pct Recovery = 25% Analysis Date = 01/09/15 Pct Recovery = 25% Analysis Date = 12/30/14 Pct Recovery = 25% Analysis Date = 12/30/14 Pct Recovery = 25% Analysis Date = 12/20/14 Pct Recovery = 25% Analysis Date = 12/20/14 Pct Recovery = 25% Analysis Date = 12/11/14 Pct Recovery = 25% Analysis Date = 12/11/14 Pct Recovery = 25% Analysis Date = 12/01/14 Pct Recovery = 26% Analysis Date = 12/01/14 Pct Recovery = 26% Analysis Date = 11/21/14 Pct Recovery = 26% Analysis Date = 11/21/14 Pct Recovery = 26% Analysis Date = 11/11/14 Pct Recovery = 26% Analysis Date = 11/11/14 Pct Recovery = 26% Analysis Date = 11/01/14 Pct Recovery = 26% Analysis Date = 11/01/14 Pct Recovery = 26% Analysis Date = 10/22/14 Pct Recovery = 26% Analysis Date = 10/22/14 Pct Recovery = 26% Analysis Date = 10/12/14 Pct Recovery = 26% Analysis Date = 10/12/14 Pct Recovery = 26% Analysis Date = 10/02/14 Pct Recovery = 26% Analysis Date = 10/02/14 Pct Recovery = 26% Analysis Date = 09/22/14 Pct Recovery = 26% Analysis Date = 09/22/14 Pct Recovery = 26% Analysis Date = 09/12/14 Pct Recovery = 26% Analysis Date = 09/12/14 Pct Recovery = 26% Analysis Date = 09/03/14 Pct Recovery = 26% Analysis Date = 09/03/14 Pct Recovery = 26% Analysis Date = 08/24/14 Pct Recovery = 26% Analysis Date = 08/24/14 Pct Recovery = 26% Analysis Date = 08/14/14 Pct Recovery = 26% Analysis Date = 08/14/14 Pct Recovery = 26% Analysis Date = 08/04/14 Pct Recovery = 26% Analysis Date = 08/04/14 Pct Recovery = 26% Analysis Date = 07/25/14 Pct Recovery = 26% Analysis Date = 07/25/14 Pct Recovery = 26% Analysis Date = 07/15/14 Pct Recovery = 26% Analysis Date = 07/15/14 Pct Recovery = 26% Analysis Date = 07/05/14 Pct Recovery = 26% Analysis Date = 07/05/14 Pct Recovery = 26% Analysis Date = 06/25/14 Pct Recovery = 26% Analysis Date = 06/25/14 Pct Recovery = 26% Analysis Date = 06/15/14 Pct Recovery = 26% Analysis Date = 06/15/14 Pct Recovery = 26% Analysis Date = 06/05/14 Pct Recovery = 26% Analysis Date = 06/05/14 Pct Recovery = 26% Analysis Date = 05/27/14 Pct Recovery = 26% Analysis Date = 05/27/14 Pct Recovery = 26% Analysis Date = 05/17/14 Pct Recovery = 26% Analysis Date = 05/17/14 Pct Recovery = 26% Analysis Date = 05/07/14 Pct Recovery = 26% Analysis Date = 05/07/14 Pct Recovery = 26% Analysis Date = 04/27/14 Pct Recovery = 26% Analysis Date = 04/27/14 Pct Recovery = 26% Analysis Date = 04/17/14 Pct Recovery = 26% Analysis Date = 04/17/14 Pct Recovery = 26% Analysis Date = 04/07/14 Pct Recovery = 26% Analysis Date = 04/07/14 Pct Recovery = 26% Analysis Date = 03/28/14 Pct Recovery = 26% Analysis Date = 03/28/14 Pct Recovery = 26% Analysis Date = 03/18/14 Pct Recovery = 26% Analysis Date = 03/18/14 Pct Recovery = 26% Analysis Date = 03/08/14 Pct Recovery = 26% Analysis Date = 03/08/14 Pct Recovery = 26% Analysis Date = 02/26/14 Pct Recovery = 26% Analysis Date = 02/26/14 Pct Recovery = 26% Analysis Date = 02/17/14 Pct Recovery = 26% Analysis Date = 02/17/14 Pct Recovery = 26% Analysis Date = 02/07/14 Pct Recovery = 26% Analysis Date = 02/07/14 Pct Recovery = 26% Analysis Date = 01/28/14 Pct Recovery = 26% Analysis Date = 01/28/14 Pct Recovery = 26% Analysis Date = 01/18/14 Pct Recovery = 26% Analysis Date = 01/18/14 Pct Recovery = 26% Analysis Date = 01/08/14 Pct Recovery = 26% Analysis Date = 01/08/14 Pct Recovery = 26% Analysis Date = 12/29/13 Pct Recovery = 26% Analysis Date = 12/29/13 Pct Recovery = 26% Analysis Date = 12/19/13 Pct Recovery = 26% Analysis Date = 12/19/13 Pct Recovery = 26% Analysis Date = 12/09/13 Pct Recovery = 26% Analysis Date = 12/09/13 Pct Recovery = 26% Analysis Date = 11/29/13 Pct Recovery = 26% Analysis Date = 11/29/13 Pct Recovery = 26% Analysis Date = 11/19/13 Pct Recovery = 26% Analysis Date = 11/19/13 Pct Recovery = 26% Analysis Date = 11/10/13 Pct Recovery = 26% Analysis Date = 11/10/13 Pct Recovery = 26% Analysis Date = 10/31/13 Pct Recovery = 26% Analysis Date = 10/31/13 Pct Recovery = 26% Analysis Date = 10/21/13 Pct Recovery = 25% Analysis Date = 10/21/13 Pct Recovery = 25% Analysis Date = 10/11/13 Pct Recovery = 25% Analysis Date = 10/11/13 Pct Recovery = 25% Analysis Date = 10/01/13 Pct Recovery = 25% Analysis Date = 10/01/13 Pct Recovery = 25% Analysis Date = 09/21/13 Pct Recovery = 25% Analysis Date = 09/21/13 Pct Recovery = 25% Analysis Date = 09/11/13 Pct Recovery = 25% Analysis Date = 09/11/13 Pct Recovery = 25% Analysis Date = 09/01/13 Pct Recovery = 25% Analysis Date = 09/01/13 Pct Recovery = 25% Analysis Date = 08/22/13 Pct Recovery = 25% Analysis Date = 08/22/13 Pct Recovery = 25% Analysis Date = 08/12/13 Pct Recovery = 25% Analysis Date = 08/12/13 Pct Recovery = 25% Analysis Date = 08/03/13 Pct Recovery = 25% Analysis Date = 08/03/13 Pct Recovery = 25% Analysis Date = 07/24/13 Pct Recovery = 25% Analysis Date = 07/24/13 Pct Recovery = 25% Analysis Date = 07/14/13 Pct Recovery = 25% Analysis Date = 07/14/13 Pct Recovery = 25% Analysis Date = 07/04/13 Pct Recovery = 25% Analysis Date = 07/04/13 Pct Recovery = 25% Analysis Date = 06/24/13 Pct Recovery = 25% Analysis Date = 06/24/13 Pct Recovery = 25% Analysis Date = 06/14/13 Pct Recovery = 25% Analysis Date = 06/14/13 Pct Recovery = 25% Analysis Date = 06/04/13 Pct Recovery = 25% Analysis Date = 06/04/13 Pct Recovery = 25% Analysis Date = 05/25/13 Pct Recovery = 25% Analysis Date = 05/25/13 Pct Recovery = 25% Analysis Date = 05/15/13 Pct Recovery = 25% Analysis Date = 05/15/13 Pct Recovery = 25% Analysis Date = 05/05/13 Pct Recovery = 25% Analysis Date = 05/05/13 Pct Recovery = 25% Analysis Date = 04/26/13 Pct Recovery = 25% Analysis Date = 04/26/13 Pct Recovery = 25% Analysis Date = 04/16/13 Pct Recovery = 25% Analysis Date = 04/16/13 Pct Recovery = 25% Analysis Date = 04/06/13 Pct Recovery = 25% Analysis Date = 04/06/13 Pct Recovery = 25% Analysis Date = 03/27/13 Pct Recovery = 25% Analysis Date = 03/27/13 Pct Recovery = 25% Analysis Date = 03/17/13 Pct Recovery = 24% Analysis Date = 03/17/13 Pct Recovery = 24% Analysis Date = 03/07/13 Pct Recovery = 24% Analysis Date = 03/07/13 Pct Recovery = 24% Analysis Date = 02/25/13 Pct Recovery = 24% Analysis Date = 02/25/13 Pct Recovery = 24% Analysis Date = 02/15/13 Pct Recovery = 24% Analysis Date = 02/15/13 Pct Recovery = 24% Analysis Date = 02/05/13 Pct Recovery = 24% Analysis Date = 02/05/13 Pct Recovery = 24% Analysis Date = 01/26/13 Pct Recovery = 24% Analysis Date = 01/26/13 Pct Recovery = 24% Analysis Date = 01/17/13 Pct Recovery = 24% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
DICROTOPHOS

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 70 23% 8% 23% 7%
Total 70 23% 8% 23% 7%

Sample Statistics
DICROTOPHOS

Characteristic N % % Basis
Plotted 70 96% Spiked
Estimated Values 70 96% Spiked
Deleted Values 2 2% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 73 .  
False Negatives 3 4% 3 out of 73
Not Spiked 52 .  
False Positives 0 0% 0 out of 50

OBSP Determination:
DIELDRIN
METHOD: 2033 , TESTIDCODE: 39381GCM35

Laboratory ID = 20130250061 Lab Value = 0.476 Expected Conc. = 0.5 Report level label = 0.008 Pct Recovery = 95% Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl SpecificMix = A088380 Laboratory ID = 20130810108 Lab Value = 0.196 Expected Conc. = 0.251 Report level label = 0.008 Pct Recovery = 78% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl SpecificMix = T1120530013 Laboratory ID = 20123560092 Lab Value = 0.195 Expected Conc. = 0.251 Report level label = 0.008 Pct Recovery = 78% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = T1120530013 Laboratory ID = 20140230082 Lab Value = 0.234 Expected Conc. = 0.25 Report level label = 0.008 Pct Recovery = 94% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl SpecificMix = A093651 Laboratory ID = 20132420001 Lab Value = 0.242 Expected Conc. = 0.25 Report level label = 0.008 Pct Recovery = 97% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl SpecificMix = A093651 Laboratory ID = 20130390105 Lab Value = 0.065 Expected Conc. = 0.1004 Report level label = 0.008 Pct Recovery = 64% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl SpecificMix = T1120530013 Laboratory ID = 20140860102 Lab Value = 0.070 Expected Conc. = 0.1 Report level label = 0.008 Pct Recovery = 70% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl SpecificMix = A093651 Laboratory ID = 20133400002 Lab Value = 0.100 Expected Conc. = 0.1 Report level label = 0.008 Pct Recovery = 100% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = A093651 Laboratory ID = 20132910008 Lab Value = 0.085 Expected Conc. = 0.1 Report level label = 0.008 Pct Recovery = 85% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = A093651 Laboratory ID = 20131920149 Lab Value = 0.101 Expected Conc. = 0.1 Report level label = 0.008 Pct Recovery = 101% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl SpecificMix = A093651 Laboratory ID = 20131230084 Lab Value = 0.089 Expected Conc. = 0.1 Report level label = 0.008 Pct Recovery = 89% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl SpecificMix = A088380 Laboratory ID = 20130650005 Lab Value = 0.069 Expected Conc. = 0.1 Report level label = 0.008 Pct Recovery = 69% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl SpecificMix = A088380 Laboratory ID = 20140100085 Lab Value = 0.073 Expected Conc. = 0.09 Report level label = 0.008 Pct Recovery = 82% Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl SpecificMix = T1130514013 Laboratory ID = 20132490342 Lab Value = 0.083 Expected Conc. = 0.09 Report level label = 0.008 Pct Recovery = 92% Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl SpecificMix = T1130514013 Laboratory ID = 20163370001 Lab Value = 0.084 Expected Conc. = 0.074 Report level label = 0.012 Pct Recovery = 114% Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl SpecificMix = B20160331 Laboratory ID = 20163150006 Lab Value = 0.054 Expected Conc. = 0.074 Report level label = 0.012 Pct Recovery = 73% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl SpecificMix = B20160331 Laboratory ID = 20161880109 Lab Value = 0.079 Expected Conc. = 0.074 Report level label = 0.012 Pct Recovery = 107% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl SpecificMix = 03FF076 Laboratory ID = 20171720140 Lab Value = 0.064 Expected Conc. = 0.0592 Report level label = 0.012 Pct Recovery = 109% Analysis Date = 08/31/17 SpikeMix = Supelco LC20138V: 80 µl & Phenova B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20171660002 Lab Value = 0.061 Expected Conc. = 0.0592 Report level label = 0.012 Pct Recovery = 102% Analysis Date = 08/23/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20170960001 Lab Value = 0.049 Expected Conc. = 0.0592 Report level label = 0.012 Pct Recovery = 83% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl SpecificMix = 03FF076 Laboratory ID = 20170190026 Lab Value = 0.051 Expected Conc. = 0.0592 Report level label = 0.012 Pct Recovery = 86% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20161470001 Lab Value = 0.043 Expected Conc. = 0.0592 Report level label = 0.012 Pct Recovery = 72% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20152750006 Lab Value = 0.027 Expected Conc. = 0.048 Report level label = 0.012 Pct Recovery = 55% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl SpecificMix = EN150514012 Laboratory ID = 20152460215 Lab Value = 0.031 Expected Conc. = 0.048 Report level label = 0.008 Pct Recovery = 65% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl SpecificMix = EN150514012 Laboratory ID = 20131370001 Lab Value = 0.048 Expected Conc. = 0.0475 Report level label = 0.008 Pct Recovery = 100% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl SpecificMix = 1473000 Laboratory ID = 20140370077 Lab Value = 0.038 Expected Conc. = 0.045 Report level label = 0.008 Pct Recovery = 84% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl SpecificMix = T1130514013 Laboratory ID = 20132690010 Lab Value = 0.042 Expected Conc. = 0.045 Report level label = 0.008 Pct Recovery = 93% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl SpecificMix = T1130514013 Laboratory ID = 20172230001 Lab Value = 0.038 Expected Conc. = 0.04 Report level label = 0.012 Pct Recovery = 95% Analysis Date = 10/19/17 SpikeMix = ChemService 6472100: 50 µl & Abs 071717Pest: 50 µl SpecificMix = 6472100 Laboratory ID = 20172560101 Lab Value = 0.033 Expected Conc. = 0.0399 Report level label = 0.012 Pct Recovery = 81% Analysis Date = 12/22/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6567600: 50 µl SpecificMix = EN170808006 Laboratory ID = 20172370001 Lab Value = 0.035 Expected Conc. = 0.0399 Report level label = 0.012 Pct Recovery = 88% Analysis Date = 11/18/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6537100: 50 µl SpecificMix = EN170808006 Laboratory ID = 20142720002 Lab Value = 0.027 Expected Conc. = 0.0319 Report level label = 0.008 Pct Recovery = 85% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl SpecificMix = LC06435 Laboratory ID = 20142530087 Lab Value = 0.024 Expected Conc. = 0.0319 Report level label = 0.008 Pct Recovery = 74% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl SpecificMix = LC06435 Laboratory ID = 20141570088 Lab Value = 0.016 Expected Conc. = 0.0319 Report level label = 0.008 Pct Recovery = 49% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl SpecificMix = LC06435 Laboratory ID = 20141220025 Lab Value = 0.026 Expected Conc. = 0.0319 Report level label = 0.008 Pct Recovery = 81% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl SpecificMix = LC06435 Laboratory ID = 20150720069 Lab Value = 0.033 Expected Conc. = 0.0312 Report level label = 0.008 Pct Recovery = 106% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 03DD006 Laboratory ID = 20143110108 Lab Value = 0.024 Expected Conc. = 0.0312 Report level label = 0.008 Pct Recovery = 77% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 03DD006 Laboratory ID = 20142960086 Lab Value = 0.027 Expected Conc. = 0.0312 Report level label = 0.008 Pct Recovery = 87% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 03DD006 Laboratory ID = 20142270001 Lab Value = 0.027 Expected Conc. = 0.0312 Report level label = 0.008 Pct Recovery = 88% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl SpecificMix = 03DD006 Laboratory ID = 20172020035 Lab Value = 0.030 Expected Conc. = 0.0296 Report level label = 0.012 Pct Recovery = 100% Analysis Date = 11/07/17 SpikeMix = Abs 071717Pest: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20171510080 Lab Value = 0.031 Expected Conc. = 0.0296 Report level label = 0.012 Pct Recovery = 105% Analysis Date = 06/09/17 SpikeMix = Supelco LC20138V: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20171160110 Lab Value = 0.032 Expected Conc. = 0.0296 Report level label = 0.012 Pct Recovery = 107% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = B20160331 Laboratory ID = 20170460061 Lab Value = 0.027 Expected Conc. = 0.0296 Report level label = 0.012 Pct Recovery = 93% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl SpecificMix = 03FF076 Laboratory ID = 20162660005 Lab Value = 0.026 Expected Conc. = 0.0296 Report level label = 0.012 Pct Recovery = 89% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl SpecificMix = 03FF076 Laboratory ID = 20162380004 Lab Value = 0.027 Expected Conc. = 0.0296 Report level label = 0.012 Pct Recovery = 91% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = B20160331 Laboratory ID = 20162150213 Lab Value = 0.034 Expected Conc. = 0.0296 Report level label = 0.012 Pct Recovery = 116% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl SpecificMix = B20160331 Laboratory ID = 20161600087 Lab Value = 0.024 Expected Conc. = 0.0296 Report level label = 0.012 Pct Recovery = 82% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20161340228 Lab Value = 0.024 Expected Conc. = 0.0296 Report level label = 0.012 Pct Recovery = 80% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl SpecificMix = 03FF076 Laboratory ID = 20161190075 Lab Value = 0.026 Expected Conc. = 0.0296 Report level label = 0.012 Pct Recovery = 87% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20173120093 Lab Value = 0.023 Expected Conc. = 0.024 Report level label = 0.012 Pct Recovery = 95% Analysis Date = 03/10/18 SpikeMix = ChemService 6472100: 30 µl & ChemService 6537100: 30 µl SpecificMix = 6472100 Laboratory ID = 20160630046 Lab Value = 0.018 Expected Conc. = 0.024 Report level label = 0.012 Pct Recovery = 76% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = EN150514012 Laboratory ID = 20153440001 Lab Value = 0.016 Expected Conc. = 0.024 Report level label = 0.012 Pct Recovery = 67% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = EN150514012 Laboratory ID = 20152330039 Lab Value = 0.019 Expected Conc. = 0.024 Report level label = 0.008 Pct Recovery = 80% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl SpecificMix = 041415 Laboratory ID = 20151900132 Lab Value = 0.015 Expected Conc. = 0.024 Report level label = 0.008 Pct Recovery = 62% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl SpecificMix = 041415 Laboratory ID = 20151270112 Lab Value = 0.026 Expected Conc. = 0.024 Report level label = 0.008 Pct Recovery = 108% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl SpecificMix = 041415 Laboratory ID = 20140730138 Lab Value = 0.016 Expected Conc. = 0.019 Report level label = 0.008 Pct Recovery = 85% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 1473000 Laboratory ID = 20133470008 Lab Value = 0.018 Expected Conc. = 0.019 Report level label = 0.008 Pct Recovery = 93% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl SpecificMix = 1473000 Laboratory ID = 20133310030 Lab Value = 0.023 Expected Conc. = 0.019 Report level label = 0.008 Pct Recovery = 121% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl SpecificMix = 1473000 Laboratory ID = 20131790009 Lab Value = 0.020 Expected Conc. = 0.019 Report level label = 0.008 Pct Recovery = 104% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl SpecificMix = 1473000 Laboratory ID = 20131650073 Lab Value = 0.016 Expected Conc. = 0.019 Report level label = 0.008 Pct Recovery = 82% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl SpecificMix = 1473000 Laboratory ID = 20133050050 Lab Value = 0.014 Expected Conc. = 0.018 Report level label = 0.008 Pct Recovery = 78% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl SpecificMix = T1130514013 Laboratory ID = 20132280016 Lab Value = 0.015 Expected Conc. = 0.018 Report level label = 0.008 Pct Recovery = 83% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl SpecificMix = T1130514013 Laboratory ID = 20150150115 Lab Value = 0.014 Expected Conc. = 0.016 Report level label = 0.008 Pct Recovery = 90% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl SpecificMix = LC06435 Laboratory ID = 20143370094 Lab Value = 0.013 Expected Conc. = 0.016 Report level label = 0.008 Pct Recovery = 83% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl SpecificMix = LC06435 Laboratory ID = 20141910243 Lab Value = 0.015 Expected Conc. = 0.016 Report level label = 0.008 Pct Recovery = 91% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = LC06435 Laboratory ID = 20141840097 Lab Value = 0.013 Expected Conc. = 0.016 Report level label = 0.008 Pct Recovery = 79% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl SpecificMix = LC06435 Laboratory ID = 20142200164 Lab Value = 0.016 Expected Conc. = 0.0156 Report level label = 0.008 Pct Recovery = 103% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 03DD006 Laboratory ID = 20141640076 Lab Value = 0.009 Expected Conc. = 0.0156 Report level label = 0.008 Pct Recovery = 60% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = 03DD006 Laboratory ID = 20141420140 Lab Value = 0.015 Expected Conc. = 0.0156 Report level label = 0.008 Pct Recovery = 98% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 03DD006 Laboratory ID = 20141080004 Lab Value = 0.012 Expected Conc. = 0.0156 Report level label = 0.008 Pct Recovery = 76% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl SpecificMix = 03DD006 Laboratory ID = 20161050143 Lab Value = 0.010 Expected Conc. = 0.012 Report level label = 0.012 Pct Recovery = 85% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 041415 Laboratory ID = 20160560044 Lab Value = 0.010 Expected Conc. = 0.012 Report level label = 0.012 Pct Recovery = 79% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl SpecificMix = 041415 Laboratory ID = 20160210080 Lab Value = 0.012 Expected Conc. = 0.012 Report level label = 0.012 Pct Recovery = 97% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 041415 Laboratory ID = 20160070059 Lab Value = 0.010 Expected Conc. = 0.012 Report level label = 0.012 Pct Recovery = 83% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = EN150514012 Laboratory ID = 20153160001 Lab Value = 0.010 Expected Conc. = 0.012 Report level label = 0.012 Pct Recovery = 79% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = EN150514012 Laboratory ID = 20152950078 Lab Value = 0.008 Expected Conc. = 0.012 Report level label = 0.012 Pct Recovery = 67% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 041415 Laboratory ID = 20152040177 Lab Value = 0.010 Expected Conc. = 0.012 Report level label = 0.008 Pct Recovery = 87% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl SpecificMix = 041415 Laboratory ID = 20151760208 Lab Value = 0.011 Expected Conc. = 0.012 Report level label = 0.008 Pct Recovery = 93% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl SpecificMix = EN150514012 Laboratory ID = 20151480170 Lab Value = 0.009 Expected Conc. = 0.012 Report level label = 0.008 Pct Recovery = 76% Analysis Date = 06/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150514012 Laboratory ID = 20151210037 Lab Value = 0.010 Expected Conc. = 0.012 Report level label = 0.008 Pct Recovery = 87% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 041415 Analysis Date = 03/10/18 Pct Recovery = 100% Analysis Date = 02/28/18 Pct Recovery = 100% Analysis Date = 02/28/18 Pct Recovery = 100% Analysis Date = 02/19/18 Pct Recovery = 100% Analysis Date = 02/19/18 Pct Recovery = 100% Analysis Date = 02/09/18 Pct Recovery = 100% Analysis Date = 02/09/18 Pct Recovery = 100% Analysis Date = 01/31/18 Pct Recovery = 99% Analysis Date = 01/31/18 Pct Recovery = 99% Analysis Date = 01/22/18 Pct Recovery = 99% Analysis Date = 01/22/18 Pct Recovery = 99% Analysis Date = 01/12/18 Pct Recovery = 99% Analysis Date = 01/12/18 Pct Recovery = 99% Analysis Date = 01/03/18 Pct Recovery = 99% Analysis Date = 01/03/18 Pct Recovery = 99% Analysis Date = 12/24/17 Pct Recovery = 98% Analysis Date = 12/24/17 Pct Recovery = 98% Analysis Date = 12/15/17 Pct Recovery = 98% Analysis Date = 12/15/17 Pct Recovery = 98% Analysis Date = 12/06/17 Pct Recovery = 98% Analysis Date = 12/06/17 Pct Recovery = 98% Analysis Date = 11/26/17 Pct Recovery = 98% Analysis Date = 11/26/17 Pct Recovery = 98% Analysis Date = 11/17/17 Pct Recovery = 98% Analysis Date = 11/17/17 Pct Recovery = 98% Analysis Date = 11/07/17 Pct Recovery = 97% Analysis Date = 11/07/17 Pct Recovery = 97% Analysis Date = 10/29/17 Pct Recovery = 97% Analysis Date = 10/29/17 Pct Recovery = 97% Analysis Date = 10/20/17 Pct Recovery = 97% Analysis Date = 10/20/17 Pct Recovery = 97% Analysis Date = 10/10/17 Pct Recovery = 97% Analysis Date = 10/10/17 Pct Recovery = 97% Analysis Date = 10/01/17 Pct Recovery = 96% Analysis Date = 10/01/17 Pct Recovery = 96% Analysis Date = 09/21/17 Pct Recovery = 96% Analysis Date = 09/21/17 Pct Recovery = 96% Analysis Date = 09/12/17 Pct Recovery = 96% Analysis Date = 09/12/17 Pct Recovery = 96% Analysis Date = 09/03/17 Pct Recovery = 96% Analysis Date = 09/03/17 Pct Recovery = 96% Analysis Date = 08/24/17 Pct Recovery = 96% Analysis Date = 08/24/17 Pct Recovery = 96% Analysis Date = 08/15/17 Pct Recovery = 95% Analysis Date = 08/15/17 Pct Recovery = 95% Analysis Date = 08/05/17 Pct Recovery = 95% Analysis Date = 08/05/17 Pct Recovery = 95% Analysis Date = 07/27/17 Pct Recovery = 95% Analysis Date = 07/27/17 Pct Recovery = 95% Analysis Date = 07/18/17 Pct Recovery = 95% Analysis Date = 07/18/17 Pct Recovery = 95% Analysis Date = 07/08/17 Pct Recovery = 94% Analysis Date = 07/08/17 Pct Recovery = 94% Analysis Date = 06/29/17 Pct Recovery = 94% Analysis Date = 06/29/17 Pct Recovery = 94% Analysis Date = 06/19/17 Pct Recovery = 94% Analysis Date = 06/19/17 Pct Recovery = 94% Analysis Date = 06/10/17 Pct Recovery = 94% Analysis Date = 06/10/17 Pct Recovery = 94% Analysis Date = 06/01/17 Pct Recovery = 94% Analysis Date = 06/01/17 Pct Recovery = 94% Analysis Date = 05/22/17 Pct Recovery = 93% Analysis Date = 05/22/17 Pct Recovery = 93% Analysis Date = 05/13/17 Pct Recovery = 93% Analysis Date = 05/13/17 Pct Recovery = 93% Analysis Date = 05/03/17 Pct Recovery = 93% Analysis Date = 05/03/17 Pct Recovery = 93% Analysis Date = 04/24/17 Pct Recovery = 93% Analysis Date = 04/24/17 Pct Recovery = 93% Analysis Date = 04/15/17 Pct Recovery = 93% Analysis Date = 04/15/17 Pct Recovery = 93% Analysis Date = 04/05/17 Pct Recovery = 92% Analysis Date = 04/05/17 Pct Recovery = 92% Analysis Date = 03/27/17 Pct Recovery = 92% Analysis Date = 03/27/17 Pct Recovery = 92% Analysis Date = 03/17/17 Pct Recovery = 92% Analysis Date = 03/17/17 Pct Recovery = 92% Analysis Date = 03/08/17 Pct Recovery = 92% Analysis Date = 03/08/17 Pct Recovery = 92% Analysis Date = 02/27/17 Pct Recovery = 91% Analysis Date = 02/27/17 Pct Recovery = 91% Analysis Date = 02/17/17 Pct Recovery = 91% Analysis Date = 02/17/17 Pct Recovery = 91% Analysis Date = 02/08/17 Pct Recovery = 91% Analysis Date = 02/08/17 Pct Recovery = 91% Analysis Date = 01/29/17 Pct Recovery = 91% Analysis Date = 01/29/17 Pct Recovery = 91% Analysis Date = 01/20/17 Pct Recovery = 91% Analysis Date = 01/20/17 Pct Recovery = 91% Analysis Date = 01/11/17 Pct Recovery = 90% Analysis Date = 01/11/17 Pct Recovery = 90% Analysis Date = 01/01/17 Pct Recovery = 90% Analysis Date = 01/01/17 Pct Recovery = 90% Analysis Date = 12/23/16 Pct Recovery = 90% Analysis Date = 12/23/16 Pct Recovery = 90% Analysis Date = 12/13/16 Pct Recovery = 90% Analysis Date = 12/13/16 Pct Recovery = 90% Analysis Date = 12/04/16 Pct Recovery = 90% Analysis Date = 12/04/16 Pct Recovery = 90% Analysis Date = 11/25/16 Pct Recovery = 89% Analysis Date = 11/25/16 Pct Recovery = 89% Analysis Date = 11/15/16 Pct Recovery = 89% Analysis Date = 11/15/16 Pct Recovery = 89% Analysis Date = 11/06/16 Pct Recovery = 89% Analysis Date = 11/06/16 Pct Recovery = 89% Analysis Date = 10/27/16 Pct Recovery = 89% Analysis Date = 10/27/16 Pct Recovery = 89% Analysis Date = 10/18/16 Pct Recovery = 89% Analysis Date = 10/18/16 Pct Recovery = 89% Analysis Date = 10/09/16 Pct Recovery = 88% Analysis Date = 10/09/16 Pct Recovery = 88% Analysis Date = 09/29/16 Pct Recovery = 88% Analysis Date = 09/29/16 Pct Recovery = 88% Analysis Date = 09/20/16 Pct Recovery = 88% Analysis Date = 09/20/16 Pct Recovery = 88% Analysis Date = 09/10/16 Pct Recovery = 88% Analysis Date = 09/10/16 Pct Recovery = 88% Analysis Date = 09/01/16 Pct Recovery = 88% Analysis Date = 09/01/16 Pct Recovery = 88% Analysis Date = 08/23/16 Pct Recovery = 87% Analysis Date = 08/23/16 Pct Recovery = 87% Analysis Date = 08/13/16 Pct Recovery = 87% Analysis Date = 08/13/16 Pct Recovery = 87% Analysis Date = 08/04/16 Pct Recovery = 87% Analysis Date = 08/04/16 Pct Recovery = 87% Analysis Date = 07/25/16 Pct Recovery = 87% Analysis Date = 07/25/16 Pct Recovery = 87% Analysis Date = 07/16/16 Pct Recovery = 87% Analysis Date = 07/16/16 Pct Recovery = 87% Analysis Date = 07/07/16 Pct Recovery = 86% Analysis Date = 07/07/16 Pct Recovery = 86% Analysis Date = 06/27/16 Pct Recovery = 86% Analysis Date = 06/27/16 Pct Recovery = 86% Analysis Date = 06/18/16 Pct Recovery = 86% Analysis Date = 06/18/16 Pct Recovery = 86% Analysis Date = 06/08/16 Pct Recovery = 86% Analysis Date = 06/08/16 Pct Recovery = 86% Analysis Date = 05/30/16 Pct Recovery = 86% Analysis Date = 05/30/16 Pct Recovery = 86% Analysis Date = 05/21/16 Pct Recovery = 85% Analysis Date = 05/21/16 Pct Recovery = 85% Analysis Date = 05/11/16 Pct Recovery = 85% Analysis Date = 05/11/16 Pct Recovery = 85% Analysis Date = 05/02/16 Pct Recovery = 85% Analysis Date = 05/02/16 Pct Recovery = 85% Analysis Date = 04/22/16 Pct Recovery = 85% Analysis Date = 04/22/16 Pct Recovery = 85% Analysis Date = 04/13/16 Pct Recovery = 85% Analysis Date = 04/13/16 Pct Recovery = 85% Analysis Date = 04/04/16 Pct Recovery = 84% Analysis Date = 04/04/16 Pct Recovery = 84% Analysis Date = 03/25/16 Pct Recovery = 84% Analysis Date = 03/25/16 Pct Recovery = 84% Analysis Date = 03/16/16 Pct Recovery = 84% Analysis Date = 03/16/16 Pct Recovery = 84% Analysis Date = 03/06/16 Pct Recovery = 84% Analysis Date = 03/06/16 Pct Recovery = 84% Analysis Date = 02/26/16 Pct Recovery = 84% Analysis Date = 02/26/16 Pct Recovery = 84% Analysis Date = 02/17/16 Pct Recovery = 83% Analysis Date = 02/17/16 Pct Recovery = 83% Analysis Date = 02/07/16 Pct Recovery = 83% Analysis Date = 02/07/16 Pct Recovery = 83% Analysis Date = 01/29/16 Pct Recovery = 83% Analysis Date = 01/29/16 Pct Recovery = 83% Analysis Date = 01/19/16 Pct Recovery = 83% Analysis Date = 01/19/16 Pct Recovery = 83% Analysis Date = 01/10/16 Pct Recovery = 83% Analysis Date = 01/10/16 Pct Recovery = 83% Analysis Date = 01/01/16 Pct Recovery = 83% Analysis Date = 01/01/16 Pct Recovery = 83% Analysis Date = 12/22/15 Pct Recovery = 83% Analysis Date = 12/22/15 Pct Recovery = 83% Analysis Date = 12/13/15 Pct Recovery = 83% Analysis Date = 12/13/15 Pct Recovery = 83% Analysis Date = 12/03/15 Pct Recovery = 83% Analysis Date = 12/03/15 Pct Recovery = 83% Analysis Date = 11/24/15 Pct Recovery = 83% Analysis Date = 11/24/15 Pct Recovery = 83% Analysis Date = 11/15/15 Pct Recovery = 83% Analysis Date = 11/15/15 Pct Recovery = 83% Analysis Date = 11/05/15 Pct Recovery = 83% Analysis Date = 11/05/15 Pct Recovery = 83% Analysis Date = 10/27/15 Pct Recovery = 82% Analysis Date = 10/27/15 Pct Recovery = 82% Analysis Date = 10/17/15 Pct Recovery = 82% Analysis Date = 10/17/15 Pct Recovery = 82% Analysis Date = 10/08/15 Pct Recovery = 82% Analysis Date = 10/08/15 Pct Recovery = 82% Analysis Date = 09/29/15 Pct Recovery = 82% Analysis Date = 09/29/15 Pct Recovery = 82% Analysis Date = 09/19/15 Pct Recovery = 82% Analysis Date = 09/19/15 Pct Recovery = 82% Analysis Date = 09/10/15 Pct Recovery = 82% Analysis Date = 09/10/15 Pct Recovery = 82% Analysis Date = 08/31/15 Pct Recovery = 82% Analysis Date = 08/31/15 Pct Recovery = 82% Analysis Date = 08/22/15 Pct Recovery = 82% Analysis Date = 08/22/15 Pct Recovery = 82% Analysis Date = 08/13/15 Pct Recovery = 82% Analysis Date = 08/13/15 Pct Recovery = 82% Analysis Date = 08/03/15 Pct Recovery = 82% Analysis Date = 08/03/15 Pct Recovery = 82% Analysis Date = 07/25/15 Pct Recovery = 82% Analysis Date = 07/25/15 Pct Recovery = 82% Analysis Date = 07/15/15 Pct Recovery = 82% Analysis Date = 07/15/15 Pct Recovery = 82% Analysis Date = 07/06/15 Pct Recovery = 82% Analysis Date = 07/06/15 Pct Recovery = 82% Analysis Date = 06/27/15 Pct Recovery = 82% Analysis Date = 06/27/15 Pct Recovery = 82% Analysis Date = 06/17/15 Pct Recovery = 82% Analysis Date = 06/17/15 Pct Recovery = 82% Analysis Date = 06/08/15 Pct Recovery = 82% Analysis Date = 06/08/15 Pct Recovery = 82% Analysis Date = 05/29/15 Pct Recovery = 82% Analysis Date = 05/29/15 Pct Recovery = 82% Analysis Date = 05/20/15 Pct Recovery = 82% Analysis Date = 05/20/15 Pct Recovery = 82% Analysis Date = 05/11/15 Pct Recovery = 82% Analysis Date = 05/11/15 Pct Recovery = 82% Analysis Date = 05/01/15 Pct Recovery = 82% Analysis Date = 05/01/15 Pct Recovery = 82% Analysis Date = 04/22/15 Pct Recovery = 82% Analysis Date = 04/22/15 Pct Recovery = 82% Analysis Date = 04/12/15 Pct Recovery = 82% Analysis Date = 04/12/15 Pct Recovery = 82% Analysis Date = 04/03/15 Pct Recovery = 82% Analysis Date = 04/03/15 Pct Recovery = 82% Analysis Date = 03/25/15 Pct Recovery = 82% Analysis Date = 03/25/15 Pct Recovery = 82% Analysis Date = 03/15/15 Pct Recovery = 82% Analysis Date = 03/15/15 Pct Recovery = 82% Analysis Date = 03/06/15 Pct Recovery = 82% Analysis Date = 03/06/15 Pct Recovery = 82% Analysis Date = 02/24/15 Pct Recovery = 82% Analysis Date = 02/24/15 Pct Recovery = 82% Analysis Date = 02/15/15 Pct Recovery = 83% Analysis Date = 02/15/15 Pct Recovery = 83% Analysis Date = 02/06/15 Pct Recovery = 83% Analysis Date = 02/06/15 Pct Recovery = 83% Analysis Date = 01/27/15 Pct Recovery = 83% Analysis Date = 01/27/15 Pct Recovery = 83% Analysis Date = 01/18/15 Pct Recovery = 83% Analysis Date = 01/18/15 Pct Recovery = 83% Analysis Date = 01/08/15 Pct Recovery = 83% Analysis Date = 01/08/15 Pct Recovery = 83% Analysis Date = 12/30/14 Pct Recovery = 83% Analysis Date = 12/30/14 Pct Recovery = 83% Analysis Date = 12/21/14 Pct Recovery = 83% Analysis Date = 12/21/14 Pct Recovery = 83% Analysis Date = 12/11/14 Pct Recovery = 83% Analysis Date = 12/11/14 Pct Recovery = 83% Analysis Date = 12/02/14 Pct Recovery = 84% Analysis Date = 12/02/14 Pct Recovery = 84% Analysis Date = 11/22/14 Pct Recovery = 84% Analysis Date = 11/22/14 Pct Recovery = 84% Analysis Date = 11/13/14 Pct Recovery = 84% Analysis Date = 11/13/14 Pct Recovery = 84% Analysis Date = 11/04/14 Pct Recovery = 84% Analysis Date = 11/04/14 Pct Recovery = 84% Analysis Date = 10/25/14 Pct Recovery = 84% Analysis Date = 10/25/14 Pct Recovery = 84% Analysis Date = 10/16/14 Pct Recovery = 84% Analysis Date = 10/16/14 Pct Recovery = 84% Analysis Date = 10/06/14 Pct Recovery = 84% Analysis Date = 10/06/14 Pct Recovery = 84% Analysis Date = 09/27/14 Pct Recovery = 84% Analysis Date = 09/27/14 Pct Recovery = 84% Analysis Date = 09/18/14 Pct Recovery = 85% Analysis Date = 09/18/14 Pct Recovery = 85% Analysis Date = 09/08/14 Pct Recovery = 85% Analysis Date = 09/08/14 Pct Recovery = 85% Analysis Date = 08/30/14 Pct Recovery = 85% Analysis Date = 08/30/14 Pct Recovery = 85% Analysis Date = 08/20/14 Pct Recovery = 85% Analysis Date = 08/20/14 Pct Recovery = 85% Analysis Date = 08/11/14 Pct Recovery = 85% Analysis Date = 08/11/14 Pct Recovery = 85% Analysis Date = 08/02/14 Pct Recovery = 85% Analysis Date = 08/02/14 Pct Recovery = 85% Analysis Date = 07/23/14 Pct Recovery = 85% Analysis Date = 07/23/14 Pct Recovery = 85% Analysis Date = 07/14/14 Pct Recovery = 85% Analysis Date = 07/14/14 Pct Recovery = 85% Analysis Date = 07/04/14 Pct Recovery = 85% Analysis Date = 07/04/14 Pct Recovery = 85% Analysis Date = 06/25/14 Pct Recovery = 85% Analysis Date = 06/25/14 Pct Recovery = 85% Analysis Date = 06/16/14 Pct Recovery = 85% Analysis Date = 06/16/14 Pct Recovery = 85% Analysis Date = 06/06/14 Pct Recovery = 86% Analysis Date = 06/06/14 Pct Recovery = 86% Analysis Date = 05/28/14 Pct Recovery = 86% Analysis Date = 05/28/14 Pct Recovery = 86% Analysis Date = 05/18/14 Pct Recovery = 86% Analysis Date = 05/18/14 Pct Recovery = 86% Analysis Date = 05/09/14 Pct Recovery = 86% Analysis Date = 05/09/14 Pct Recovery = 86% Analysis Date = 04/30/14 Pct Recovery = 86% Analysis Date = 04/30/14 Pct Recovery = 86% Analysis Date = 04/20/14 Pct Recovery = 86% Analysis Date = 04/20/14 Pct Recovery = 86% Analysis Date = 04/11/14 Pct Recovery = 86% Analysis Date = 04/11/14 Pct Recovery = 86% Analysis Date = 04/01/14 Pct Recovery = 86% Analysis Date = 04/01/14 Pct Recovery = 86% Analysis Date = 03/23/14 Pct Recovery = 86% Analysis Date = 03/23/14 Pct Recovery = 86% Analysis Date = 03/14/14 Pct Recovery = 86% Analysis Date = 03/14/14 Pct Recovery = 86% Analysis Date = 03/04/14 Pct Recovery = 86% Analysis Date = 03/04/14 Pct Recovery = 86% Analysis Date = 02/23/14 Pct Recovery = 86% Analysis Date = 02/23/14 Pct Recovery = 86% Analysis Date = 02/13/14 Pct Recovery = 86% Analysis Date = 02/13/14 Pct Recovery = 86% Analysis Date = 02/04/14 Pct Recovery = 86% Analysis Date = 02/04/14 Pct Recovery = 86% Analysis Date = 01/26/14 Pct Recovery = 86% Analysis Date = 01/26/14 Pct Recovery = 86% Analysis Date = 01/16/14 Pct Recovery = 86% Analysis Date = 01/16/14 Pct Recovery = 86% Analysis Date = 01/07/14 Pct Recovery = 86% Analysis Date = 01/07/14 Pct Recovery = 86% Analysis Date = 12/28/13 Pct Recovery = 86% Analysis Date = 12/28/13 Pct Recovery = 86% Analysis Date = 12/19/13 Pct Recovery = 86% Analysis Date = 12/19/13 Pct Recovery = 86% Analysis Date = 12/10/13 Pct Recovery = 86% Analysis Date = 12/10/13 Pct Recovery = 86% Analysis Date = 11/30/13 Pct Recovery = 86% Analysis Date = 11/30/13 Pct Recovery = 86% Analysis Date = 11/21/13 Pct Recovery = 86% Analysis Date = 11/21/13 Pct Recovery = 86% Analysis Date = 11/11/13 Pct Recovery = 86% Analysis Date = 11/11/13 Pct Recovery = 86% Analysis Date = 11/02/13 Pct Recovery = 86% Analysis Date = 11/02/13 Pct Recovery = 86% Analysis Date = 10/24/13 Pct Recovery = 87% Analysis Date = 10/24/13 Pct Recovery = 87% Analysis Date = 10/14/13 Pct Recovery = 87% Analysis Date = 10/14/13 Pct Recovery = 87% Analysis Date = 10/05/13 Pct Recovery = 87% Analysis Date = 10/05/13 Pct Recovery = 87% Analysis Date = 09/25/13 Pct Recovery = 87% Analysis Date = 09/25/13 Pct Recovery = 87% Analysis Date = 09/16/13 Pct Recovery = 87% Analysis Date = 09/16/13 Pct Recovery = 87% Analysis Date = 09/07/13 Pct Recovery = 87% Analysis Date = 09/07/13 Pct Recovery = 87% Analysis Date = 08/28/13 Pct Recovery = 87% Analysis Date = 08/28/13 Pct Recovery = 87% Analysis Date = 08/19/13 Pct Recovery = 87% Analysis Date = 08/19/13 Pct Recovery = 87% Analysis Date = 08/09/13 Pct Recovery = 87% Analysis Date = 08/09/13 Pct Recovery = 87% Analysis Date = 07/31/13 Pct Recovery = 87% Analysis Date = 07/31/13 Pct Recovery = 87% Analysis Date = 07/22/13 Pct Recovery = 87% Analysis Date = 07/22/13 Pct Recovery = 87% Analysis Date = 07/12/13 Pct Recovery = 87% Analysis Date = 07/12/13 Pct Recovery = 87% Analysis Date = 07/03/13 Pct Recovery = 87% Analysis Date = 07/03/13 Pct Recovery = 87% Analysis Date = 06/23/13 Pct Recovery = 87% Analysis Date = 06/23/13 Pct Recovery = 87% Analysis Date = 06/14/13 Pct Recovery = 87% Analysis Date = 06/14/13 Pct Recovery = 87% Analysis Date = 06/05/13 Pct Recovery = 87% Analysis Date = 06/05/13 Pct Recovery = 87% Analysis Date = 05/26/13 Pct Recovery = 87% Analysis Date = 05/26/13 Pct Recovery = 87% Analysis Date = 05/17/13 Pct Recovery = 87% Analysis Date = 05/17/13 Pct Recovery = 87% Analysis Date = 05/07/13 Pct Recovery = 87% Analysis Date = 05/07/13 Pct Recovery = 87% Analysis Date = 04/28/13 Pct Recovery = 87% Analysis Date = 04/28/13 Pct Recovery = 87% Analysis Date = 04/19/13 Pct Recovery = 87% Analysis Date = 04/19/13 Pct Recovery = 87% Analysis Date = 04/09/13 Pct Recovery = 87% Analysis Date = 04/09/13 Pct Recovery = 87% Analysis Date = 03/31/13 Pct Recovery = 87% Analysis Date = 03/31/13 Pct Recovery = 87% Analysis Date = 03/21/13 Pct Recovery = 87% Analysis Date = 03/21/13 Pct Recovery = 87% Analysis Date = 03/12/13 Pct Recovery = 87% Analysis Date = 03/12/13 Pct Recovery = 87% Analysis Date = 03/03/13 Pct Recovery = 87% Analysis Date = 03/03/13 Pct Recovery = 87% Analysis Date = 02/21/13 Pct Recovery = 87% Analysis Date = 02/21/13 Pct Recovery = 87% Analysis Date = 02/12/13 Pct Recovery = 87% Analysis Date = 02/12/13 Pct Recovery = 87% Analysis Date = 02/02/13 Pct Recovery = 87% Analysis Date = 02/02/13 Pct Recovery = 87% Analysis Date = 01/24/13 Pct Recovery = 87% Analysis Date = 01/24/13 Pct Recovery = 87% Analysis Date = 01/15/13 Pct Recovery = 87% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
DIELDRIN

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 79 87% 14% 86% 13%
Total 79 87% 14% 86% 13%

Sample Statistics
DIELDRIN

Characteristic N % % Basis
Plotted 79 100% Spiked
Estimated Values 3 4% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 79 .  
False Negatives 0 0% 0 out of 79
Not Spiked 39 .  
False Positives 1 3% 1 out of 39

OBSP Determination:
DIMETHOATE
METHOD: 2033 , TESTIDCODE: 82662GCM40

Laboratory ID = 20140100085 Lab Value = 0.041 Expected Conc. = 0.15 Report level label = 0.01 Pct Recovery = 27% Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl SpecificMix = T1130514013 Laboratory ID = 20132490342 Lab Value = 0.043 Expected Conc. = 0.15 Report level label = 0.01 Pct Recovery = 29% Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl SpecificMix = T1130514013 Laboratory ID = 20130810108 Lab Value = 0.044 Expected Conc. = 0.1252 Report level label = 0.01 Pct Recovery = 35% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl SpecificMix = LB92783 Laboratory ID = 20130100066 Lab Value = 0.048 Expected Conc. = 0.1252 Report level label = 0.01 Pct Recovery = 38% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl SpecificMix = LB92783 Laboratory ID = 20130940097 Lab Value = 0.041 Expected Conc. = 0.125 Report level label = 0.01 Pct Recovery = 32% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = 0507-12-04.2 Laboratory ID = 20123560092 Lab Value = 0.045 Expected Conc. = 0.125 Report level label = 0.01 Pct Recovery = 36% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = 0507-12-04.2 Laboratory ID = 20140370077 Lab Value = 0.021 Expected Conc. = 0.075 Report level label = 0.01 Pct Recovery = 28% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl SpecificMix = T1130514013 Laboratory ID = 20132690010 Lab Value = 0.035 Expected Conc. = 0.075 Report level label = 0.01 Pct Recovery = 47% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl SpecificMix = T1130514013 Laboratory ID = 20131370001 Lab Value = 0.037 Expected Conc. = 0.075 Report level label = 0.01 Pct Recovery = 50% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl SpecificMix = 1473000 Laboratory ID = 20172510330 Lab Value = 0.021 Expected Conc. = 0.067 Report level label = 0.01 Pct Recovery = 32% Analysis Date = 12/29/17 SpikeMix = ChemService 6537100: 100 µl & Abs 071817Pest: 100 µl SpecificMix = 071817Pest Laboratory ID = 20162860079 Lab Value = 0.022 Expected Conc. = 0.063 Report level label = 0.01 Pct Recovery = 34% Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl SpecificMix = 060916 Laboratory ID = 20163150006 Lab Value = 0.019 Expected Conc. = 0.063 Report level label = 0.01 Pct Recovery = 30% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl SpecificMix = 060916 Laboratory ID = 20152460215 Lab Value = 0.016 Expected Conc. = 0.0597 Report level label = 0.01 Pct Recovery = 27% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl SpecificMix = 0406-15-01 Laboratory ID = 20171660002 Lab Value = 0.016 Expected Conc. = 0.0504 Report level label = 0.01 Pct Recovery = 31% Analysis Date = 08/23/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = 060916 Laboratory ID = 20171380001 Lab Value = 0.013 Expected Conc. = 0.0504 Report level label = 0.01 Pct Recovery = 26% Analysis Date = 06/07/17 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 041816 Laboratory ID = 20170190026 Lab Value = 0.013 Expected Conc. = 0.0504 Report level label = 0.01 Pct Recovery = 25% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = 060916 Laboratory ID = 20161740258 Lab Value = 0.012 Expected Conc. = 0.0504 Report level label = 0.01 Pct Recovery = 24% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 041816 Laboratory ID = 20130390105 Lab Value = 0.016 Expected Conc. = 0.0501 Report level label = 0.01 Pct Recovery = 33% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl SpecificMix = LB92783 Laboratory ID = 20130510051 Lab Value = 0.023 Expected Conc. = 0.05 Report level label = 0.01 Pct Recovery = 47% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl SpecificMix = 0507-12-04.2 Laboratory ID = 20150430092 Lab Value = 0.004 Expected Conc. = 0.0403 Report level label = 0.01 Pct Recovery = 10% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl SpecificMix = E1140407002 Laboratory ID = 20143110108 Lab Value = 0.013 Expected Conc. = 0.0403 Report level label = 0.01 Pct Recovery = 33% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl SpecificMix = E1140407002 Laboratory ID = 20142720002 Lab Value = 0.012 Expected Conc. = 0.0403 Report level label = 0.01 Pct Recovery = 29% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl SpecificMix = E1140407002 Laboratory ID = 20141770149 Lab Value = 0.013 Expected Conc. = 0.0403 Report level label = 0.01 Pct Recovery = 31% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl SpecificMix = E1140407002 Laboratory ID = 20143240095 Lab Value = 0.017 Expected Conc. = 0.0402 Report level label = 0.01 Pct Recovery = 42% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl SpecificMix = 032714 Laboratory ID = 20142270001 Lab Value = 0.013 Expected Conc. = 0.0402 Report level label = 0.01 Pct Recovery = 33% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl SpecificMix = 032714 Laboratory ID = 20141220025 Lab Value = 0.017 Expected Conc. = 0.0402 Report level label = 0.01 Pct Recovery = 42% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl SpecificMix = 032714 Laboratory ID = 20172560101 Lab Value = 0.014 Expected Conc. = 0.035 Report level label = 0.01 Pct Recovery = 39% Analysis Date = 12/22/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6567600: 50 µl SpecificMix = 6567600 Laboratory ID = 20161260151 Lab Value = 0.011 Expected Conc. = 0.032 Report level label = 0.01 Pct Recovery = 35% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = 3851600 Laboratory ID = 20151550293 Lab Value = 0.014 Expected Conc. = 0.032 Report level label = 0.01 Pct Recovery = 44% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl SpecificMix = 3851600 Laboratory ID = 20151270112 Lab Value = 0.015 Expected Conc. = 0.032 Report level label = 0.01 Pct Recovery = 48% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl SpecificMix = 3851600 Laboratory ID = 20133470008 Lab Value = 0.012 Expected Conc. = 0.03 Report level label = 0.01 Pct Recovery = 39% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl SpecificMix = 1473000 Laboratory ID = 20133310030 Lab Value = 0.016 Expected Conc. = 0.03 Report level label = 0.01 Pct Recovery = 52% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl SpecificMix = 1473000 Laboratory ID = 20133050050 Lab Value = 0.016 Expected Conc. = 0.03 Report level label = 0.01 Pct Recovery = 52% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl SpecificMix = T1130514013 Laboratory ID = 20132280016 Lab Value = 0.021 Expected Conc. = 0.03 Report level label = 0.01 Pct Recovery = 69% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl SpecificMix = T1130514013 Laboratory ID = 20131790009 Lab Value = 0.021 Expected Conc. = 0.03 Report level label = 0.01 Pct Recovery = 68% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl SpecificMix = 1473000 Laboratory ID = 20131650073 Lab Value = 0.021 Expected Conc. = 0.03 Report level label = 0.01 Pct Recovery = 69% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl SpecificMix = 1473000 Laboratory ID = 20160770090 Lab Value = 0.012 Expected Conc. = 0.0298 Report level label = 0.01 Pct Recovery = 42% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20160630046 Lab Value = 0.011 Expected Conc. = 0.0298 Report level label = 0.01 Pct Recovery = 36% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20153510109 Lab Value = 0.010 Expected Conc. = 0.0298 Report level label = 0.01 Pct Recovery = 32% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20153440001 Lab Value = 0.010 Expected Conc. = 0.0298 Report level label = 0.01 Pct Recovery = 32% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20171940002 Lab Value = 0.012 Expected Conc. = 0.0252 Report level label = 0.01 Pct Recovery = 46% Analysis Date = 11/10/17 SpikeMix = ChemService 5054800: 40 µl & NSI 041816: 40 µl SpecificMix = 041816 Laboratory ID = 20171160110 Lab Value = 0.009 Expected Conc. = 0.0252 Report level label = 0.01 Pct Recovery = 36% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = 060916 Laboratory ID = 20162520001 Lab Value = 0.014 Expected Conc. = 0.0252 Report level label = 0.01 Pct Recovery = 57% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl SpecificMix = 060916 Laboratory ID = 20162380004 Lab Value = 0.013 Expected Conc. = 0.0252 Report level label = 0.01 Pct Recovery = 51% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = 060916 Laboratory ID = 20162020124 Lab Value = 0.011 Expected Conc. = 0.0252 Report level label = 0.01 Pct Recovery = 42% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl SpecificMix = 041816 Laboratory ID = 20161600087 Lab Value = 0.010 Expected Conc. = 0.0252 Report level label = 0.01 Pct Recovery = 38% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 041816 Laboratory ID = 20161340228 Lab Value = 0.009 Expected Conc. = 0.0252 Report level label = 0.01 Pct Recovery = 35% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl SpecificMix = 041816 Laboratory ID = 20161190075 Lab Value = 0.010 Expected Conc. = 0.0252 Report level label = 0.01 Pct Recovery = 38% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 041816 Laboratory ID = 20142470041 Lab Value = 0.010 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 48% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141910243 Lab Value = 0.008 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 37% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141640076 Lab Value = 0.009 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 44% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141360094 Lab Value = 0.009 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 44% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = E1140407002 Laboratory ID = 20172780018 Lab Value = 0.007 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 37% Analysis Date = 02/08/18 SpikeMix = ChemService 6537100: 30 µl & Abs 071817Pest: 30 µl SpecificMix = 071817Pest Laboratory ID = 20150150115 Lab Value = 0.010 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 49% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl SpecificMix = 032714 Laboratory ID = 20142820151 Lab Value = 0.009 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 46% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl SpecificMix = 032714 Laboratory ID = 20141490205 Lab Value = 0.011 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 54% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = 032714 Laboratory ID = 20141080004 Lab Value = 0.009 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 43% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl SpecificMix = 032714 Laboratory ID = 20160430111 Lab Value = 0.009 Expected Conc. = 0.016 Report level label = 0.01 Pct Recovery = 57% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 3851600 Laboratory ID = 20160210080 Lab Value = 0.007 Expected Conc. = 0.016 Report level label = 0.01 Pct Recovery = 46% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 3851600 Laboratory ID = 20152950078 Lab Value = 0.006 Expected Conc. = 0.016 Report level label = 0.01 Pct Recovery = 36% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 3851600 Laboratory ID = 20153030068 Lab Value = 0.007 Expected Conc. = 0.016 Report level label = 0.01 Pct Recovery = 46% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = 3851600 Laboratory ID = 20151760208 Lab Value = 0.008 Expected Conc. = 0.016 Report level label = 0.01 Pct Recovery = 48% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl SpecificMix = 3851600 Laboratory ID = 20151380009 Lab Value = 0.007 Expected Conc. = 0.016 Report level label = 0.01 Pct Recovery = 46% Analysis Date = 05/30/15 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 3851600 Laboratory ID = 20152190003 Lab Value = 0.006 Expected Conc. = 0.0149 Report level label = 0.01 Pct Recovery = 38% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = 0406-15-01 Laboratory ID = 20152040177 Lab Value = 0.006 Expected Conc. = 0.0149 Report level label = 0.01 Pct Recovery = 38% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl SpecificMix = 0406-15-01 Analysis Date = 02/08/18 Pct Recovery = 36% Analysis Date = 01/29/18 Pct Recovery = 36% Analysis Date = 01/29/18 Pct Recovery = 36% Analysis Date = 01/20/18 Pct Recovery = 36% Analysis Date = 01/20/18 Pct Recovery = 36% Analysis Date = 01/11/18 Pct Recovery = 36% Analysis Date = 01/11/18 Pct Recovery = 36% Analysis Date = 01/02/18 Pct Recovery = 36% Analysis Date = 01/02/18 Pct Recovery = 36% Analysis Date = 12/23/17 Pct Recovery = 36% Analysis Date = 12/23/17 Pct Recovery = 36% Analysis Date = 12/14/17 Pct Recovery = 36% Analysis Date = 12/14/17 Pct Recovery = 36% Analysis Date = 12/05/17 Pct Recovery = 36% Analysis Date = 12/05/17 Pct Recovery = 36% Analysis Date = 11/26/17 Pct Recovery = 36% Analysis Date = 11/26/17 Pct Recovery = 36% Analysis Date = 11/16/17 Pct Recovery = 36% Analysis Date = 11/16/17 Pct Recovery = 36% Analysis Date = 11/07/17 Pct Recovery = 36% Analysis Date = 11/07/17 Pct Recovery = 36% Analysis Date = 10/29/17 Pct Recovery = 36% Analysis Date = 10/29/17 Pct Recovery = 36% Analysis Date = 10/20/17 Pct Recovery = 36% Analysis Date = 10/20/17 Pct Recovery = 36% Analysis Date = 10/10/17 Pct Recovery = 36% Analysis Date = 10/10/17 Pct Recovery = 36% Analysis Date = 10/01/17 Pct Recovery = 36% Analysis Date = 10/01/17 Pct Recovery = 36% Analysis Date = 09/22/17 Pct Recovery = 36% Analysis Date = 09/22/17 Pct Recovery = 36% Analysis Date = 09/13/17 Pct Recovery = 36% Analysis Date = 09/13/17 Pct Recovery = 36% Analysis Date = 09/03/17 Pct Recovery = 36% Analysis Date = 09/03/17 Pct Recovery = 36% Analysis Date = 08/25/17 Pct Recovery = 37% Analysis Date = 08/25/17 Pct Recovery = 37% Analysis Date = 08/16/17 Pct Recovery = 37% Analysis Date = 08/16/17 Pct Recovery = 37% Analysis Date = 08/07/17 Pct Recovery = 37% Analysis Date = 08/07/17 Pct Recovery = 37% Analysis Date = 07/28/17 Pct Recovery = 37% Analysis Date = 07/28/17 Pct Recovery = 37% Analysis Date = 07/19/17 Pct Recovery = 37% Analysis Date = 07/19/17 Pct Recovery = 37% Analysis Date = 07/10/17 Pct Recovery = 37% Analysis Date = 07/10/17 Pct Recovery = 37% Analysis Date = 07/01/17 Pct Recovery = 37% Analysis Date = 07/01/17 Pct Recovery = 37% Analysis Date = 06/21/17 Pct Recovery = 37% Analysis Date = 06/21/17 Pct Recovery = 37% Analysis Date = 06/12/17 Pct Recovery = 37% Analysis Date = 06/12/17 Pct Recovery = 37% Analysis Date = 06/03/17 Pct Recovery = 37% Analysis Date = 06/03/17 Pct Recovery = 37% Analysis Date = 05/25/17 Pct Recovery = 37% Analysis Date = 05/25/17 Pct Recovery = 37% Analysis Date = 05/15/17 Pct Recovery = 37% Analysis Date = 05/15/17 Pct Recovery = 37% Analysis Date = 05/06/17 Pct Recovery = 37% Analysis Date = 05/06/17 Pct Recovery = 37% Analysis Date = 04/27/17 Pct Recovery = 37% Analysis Date = 04/27/17 Pct Recovery = 37% Analysis Date = 04/18/17 Pct Recovery = 37% Analysis Date = 04/18/17 Pct Recovery = 37% Analysis Date = 04/08/17 Pct Recovery = 37% Analysis Date = 04/08/17 Pct Recovery = 37% Analysis Date = 03/30/17 Pct Recovery = 37% Analysis Date = 03/30/17 Pct Recovery = 37% Analysis Date = 03/21/17 Pct Recovery = 37% Analysis Date = 03/21/17 Pct Recovery = 37% Analysis Date = 03/12/17 Pct Recovery = 37% Analysis Date = 03/12/17 Pct Recovery = 37% Analysis Date = 03/02/17 Pct Recovery = 37% Analysis Date = 03/02/17 Pct Recovery = 37% Analysis Date = 02/21/17 Pct Recovery = 37% Analysis Date = 02/21/17 Pct Recovery = 37% Analysis Date = 02/12/17 Pct Recovery = 37% Analysis Date = 02/12/17 Pct Recovery = 37% Analysis Date = 02/03/17 Pct Recovery = 37% Analysis Date = 02/03/17 Pct Recovery = 37% Analysis Date = 01/24/17 Pct Recovery = 37% Analysis Date = 01/24/17 Pct Recovery = 37% Analysis Date = 01/15/17 Pct Recovery = 37% Analysis Date = 01/15/17 Pct Recovery = 37% Analysis Date = 01/06/17 Pct Recovery = 37% Analysis Date = 01/06/17 Pct Recovery = 37% Analysis Date = 12/28/16 Pct Recovery = 37% Analysis Date = 12/28/16 Pct Recovery = 37% Analysis Date = 12/18/16 Pct Recovery = 37% Analysis Date = 12/18/16 Pct Recovery = 37% Analysis Date = 12/09/16 Pct Recovery = 37% Analysis Date = 12/09/16 Pct Recovery = 37% Analysis Date = 11/30/16 Pct Recovery = 38% Analysis Date = 11/30/16 Pct Recovery = 38% Analysis Date = 11/21/16 Pct Recovery = 38% Analysis Date = 11/21/16 Pct Recovery = 38% Analysis Date = 11/11/16 Pct Recovery = 38% Analysis Date = 11/11/16 Pct Recovery = 38% Analysis Date = 11/02/16 Pct Recovery = 38% Analysis Date = 11/02/16 Pct Recovery = 38% Analysis Date = 10/24/16 Pct Recovery = 38% Analysis Date = 10/24/16 Pct Recovery = 38% Analysis Date = 10/15/16 Pct Recovery = 38% Analysis Date = 10/15/16 Pct Recovery = 38% Analysis Date = 10/05/16 Pct Recovery = 38% Analysis Date = 10/05/16 Pct Recovery = 38% Analysis Date = 09/26/16 Pct Recovery = 38% Analysis Date = 09/26/16 Pct Recovery = 38% Analysis Date = 09/17/16 Pct Recovery = 38% Analysis Date = 09/17/16 Pct Recovery = 38% Analysis Date = 09/08/16 Pct Recovery = 38% Analysis Date = 09/08/16 Pct Recovery = 38% Analysis Date = 08/29/16 Pct Recovery = 38% Analysis Date = 08/29/16 Pct Recovery = 38% Analysis Date = 08/20/16 Pct Recovery = 38% Analysis Date = 08/20/16 Pct Recovery = 38% Analysis Date = 08/11/16 Pct Recovery = 38% Analysis Date = 08/11/16 Pct Recovery = 38% Analysis Date = 08/02/16 Pct Recovery = 38% Analysis Date = 08/02/16 Pct Recovery = 38% Analysis Date = 07/23/16 Pct Recovery = 38% Analysis Date = 07/23/16 Pct Recovery = 38% Analysis Date = 07/14/16 Pct Recovery = 38% Analysis Date = 07/14/16 Pct Recovery = 38% Analysis Date = 07/05/16 Pct Recovery = 38% Analysis Date = 07/05/16 Pct Recovery = 38% Analysis Date = 06/26/16 Pct Recovery = 38% Analysis Date = 06/26/16 Pct Recovery = 38% Analysis Date = 06/16/16 Pct Recovery = 38% Analysis Date = 06/16/16 Pct Recovery = 38% Analysis Date = 06/07/16 Pct Recovery = 38% Analysis Date = 06/07/16 Pct Recovery = 38% Analysis Date = 05/29/16 Pct Recovery = 38% Analysis Date = 05/29/16 Pct Recovery = 38% Analysis Date = 05/20/16 Pct Recovery = 38% Analysis Date = 05/20/16 Pct Recovery = 38% Analysis Date = 05/10/16 Pct Recovery = 38% Analysis Date = 05/10/16 Pct Recovery = 38% Analysis Date = 05/01/16 Pct Recovery = 38% Analysis Date = 05/01/16 Pct Recovery = 38% Analysis Date = 04/22/16 Pct Recovery = 38% Analysis Date = 04/22/16 Pct Recovery = 38% Analysis Date = 04/13/16 Pct Recovery = 38% Analysis Date = 04/13/16 Pct Recovery = 38% Analysis Date = 04/03/16 Pct Recovery = 39% Analysis Date = 04/03/16 Pct Recovery = 39% Analysis Date = 03/25/16 Pct Recovery = 39% Analysis Date = 03/25/16 Pct Recovery = 39% Analysis Date = 03/16/16 Pct Recovery = 39% Analysis Date = 03/16/16 Pct Recovery = 39% Analysis Date = 03/07/16 Pct Recovery = 39% Analysis Date = 03/07/16 Pct Recovery = 39% Analysis Date = 02/26/16 Pct Recovery = 39% Analysis Date = 02/26/16 Pct Recovery = 39% Analysis Date = 02/17/16 Pct Recovery = 39% Analysis Date = 02/17/16 Pct Recovery = 39% Analysis Date = 02/08/16 Pct Recovery = 39% Analysis Date = 02/08/16 Pct Recovery = 39% Analysis Date = 01/30/16 Pct Recovery = 39% Analysis Date = 01/30/16 Pct Recovery = 39% Analysis Date = 01/20/16 Pct Recovery = 39% Analysis Date = 01/20/16 Pct Recovery = 39% Analysis Date = 01/11/16 Pct Recovery = 39% Analysis Date = 01/11/16 Pct Recovery = 39% Analysis Date = 01/02/16 Pct Recovery = 39% Analysis Date = 01/02/16 Pct Recovery = 39% Analysis Date = 12/24/15 Pct Recovery = 39% Analysis Date = 12/24/15 Pct Recovery = 39% Analysis Date = 12/14/15 Pct Recovery = 39% Analysis Date = 12/14/15 Pct Recovery = 39% Analysis Date = 12/05/15 Pct Recovery = 39% Analysis Date = 12/05/15 Pct Recovery = 39% Analysis Date = 11/26/15 Pct Recovery = 39% Analysis Date = 11/26/15 Pct Recovery = 39% Analysis Date = 11/17/15 Pct Recovery = 39% Analysis Date = 11/17/15 Pct Recovery = 39% Analysis Date = 11/07/15 Pct Recovery = 39% Analysis Date = 11/07/15 Pct Recovery = 39% Analysis Date = 10/29/15 Pct Recovery = 39% Analysis Date = 10/29/15 Pct Recovery = 39% Analysis Date = 10/20/15 Pct Recovery = 39% Analysis Date = 10/20/15 Pct Recovery = 39% Analysis Date = 10/11/15 Pct Recovery = 39% Analysis Date = 10/11/15 Pct Recovery = 39% Analysis Date = 10/01/15 Pct Recovery = 39% Analysis Date = 10/01/15 Pct Recovery = 39% Analysis Date = 09/22/15 Pct Recovery = 39% Analysis Date = 09/22/15 Pct Recovery = 39% Analysis Date = 09/13/15 Pct Recovery = 39% Analysis Date = 09/13/15 Pct Recovery = 39% Analysis Date = 09/04/15 Pct Recovery = 39% Analysis Date = 09/04/15 Pct Recovery = 39% Analysis Date = 08/25/15 Pct Recovery = 39% Analysis Date = 08/25/15 Pct Recovery = 39% Analysis Date = 08/16/15 Pct Recovery = 39% Analysis Date = 08/16/15 Pct Recovery = 39% Analysis Date = 08/07/15 Pct Recovery = 39% Analysis Date = 08/07/15 Pct Recovery = 39% Analysis Date = 07/29/15 Pct Recovery = 39% Analysis Date = 07/29/15 Pct Recovery = 39% Analysis Date = 07/19/15 Pct Recovery = 39% Analysis Date = 07/19/15 Pct Recovery = 39% Analysis Date = 07/10/15 Pct Recovery = 39% Analysis Date = 07/10/15 Pct Recovery = 39% Analysis Date = 07/01/15 Pct Recovery = 39% Analysis Date = 07/01/15 Pct Recovery = 39% Analysis Date = 06/22/15 Pct Recovery = 39% Analysis Date = 06/22/15 Pct Recovery = 39% Analysis Date = 06/12/15 Pct Recovery = 39% Analysis Date = 06/12/15 Pct Recovery = 39% Analysis Date = 06/03/15 Pct Recovery = 39% Analysis Date = 06/03/15 Pct Recovery = 39% Analysis Date = 05/25/15 Pct Recovery = 39% Analysis Date = 05/25/15 Pct Recovery = 39% Analysis Date = 05/16/15 Pct Recovery = 39% Analysis Date = 05/16/15 Pct Recovery = 39% Analysis Date = 05/06/15 Pct Recovery = 39% Analysis Date = 05/06/15 Pct Recovery = 39% Analysis Date = 04/27/15 Pct Recovery = 39% Analysis Date = 04/27/15 Pct Recovery = 39% Analysis Date = 04/18/15 Pct Recovery = 39% Analysis Date = 04/18/15 Pct Recovery = 39% Analysis Date = 04/09/15 Pct Recovery = 39% Analysis Date = 04/09/15 Pct Recovery = 39% Analysis Date = 03/30/15 Pct Recovery = 39% Analysis Date = 03/30/15 Pct Recovery = 39% Analysis Date = 03/21/15 Pct Recovery = 39% Analysis Date = 03/21/15 Pct Recovery = 39% Analysis Date = 03/12/15 Pct Recovery = 39% Analysis Date = 03/12/15 Pct Recovery = 39% Analysis Date = 03/03/15 Pct Recovery = 39% Analysis Date = 03/03/15 Pct Recovery = 39% Analysis Date = 02/21/15 Pct Recovery = 39% Analysis Date = 02/21/15 Pct Recovery = 39% Analysis Date = 02/12/15 Pct Recovery = 39% Analysis Date = 02/12/15 Pct Recovery = 39% Analysis Date = 02/03/15 Pct Recovery = 39% Analysis Date = 02/03/15 Pct Recovery = 39% Analysis Date = 01/25/15 Pct Recovery = 39% Analysis Date = 01/25/15 Pct Recovery = 39% Analysis Date = 01/15/15 Pct Recovery = 39% Analysis Date = 01/15/15 Pct Recovery = 39% Analysis Date = 01/06/15 Pct Recovery = 39% Analysis Date = 01/06/15 Pct Recovery = 39% Analysis Date = 12/28/14 Pct Recovery = 39% Analysis Date = 12/28/14 Pct Recovery = 39% Analysis Date = 12/19/14 Pct Recovery = 39% Analysis Date = 12/19/14 Pct Recovery = 39% Analysis Date = 12/09/14 Pct Recovery = 39% Analysis Date = 12/09/14 Pct Recovery = 39% Analysis Date = 11/30/14 Pct Recovery = 39% Analysis Date = 11/30/14 Pct Recovery = 39% Analysis Date = 11/21/14 Pct Recovery = 39% Analysis Date = 11/21/14 Pct Recovery = 39% Analysis Date = 11/12/14 Pct Recovery = 39% Analysis Date = 11/12/14 Pct Recovery = 39% Analysis Date = 11/02/14 Pct Recovery = 40% Analysis Date = 11/02/14 Pct Recovery = 40% Analysis Date = 10/24/14 Pct Recovery = 40% Analysis Date = 10/24/14 Pct Recovery = 40% Analysis Date = 10/15/14 Pct Recovery = 40% Analysis Date = 10/15/14 Pct Recovery = 40% Analysis Date = 10/06/14 Pct Recovery = 40% Analysis Date = 10/06/14 Pct Recovery = 40% Analysis Date = 09/26/14 Pct Recovery = 40% Analysis Date = 09/26/14 Pct Recovery = 40% Analysis Date = 09/17/14 Pct Recovery = 40% Analysis Date = 09/17/14 Pct Recovery = 40% Analysis Date = 09/08/14 Pct Recovery = 40% Analysis Date = 09/08/14 Pct Recovery = 40% Analysis Date = 08/30/14 Pct Recovery = 40% Analysis Date = 08/30/14 Pct Recovery = 40% Analysis Date = 08/20/14 Pct Recovery = 40% Analysis Date = 08/20/14 Pct Recovery = 40% Analysis Date = 08/11/14 Pct Recovery = 40% Analysis Date = 08/11/14 Pct Recovery = 40% Analysis Date = 08/02/14 Pct Recovery = 41% Analysis Date = 08/02/14 Pct Recovery = 41% Analysis Date = 07/24/14 Pct Recovery = 41% Analysis Date = 07/24/14 Pct Recovery = 41% Analysis Date = 07/14/14 Pct Recovery = 41% Analysis Date = 07/14/14 Pct Recovery = 41% Analysis Date = 07/05/14 Pct Recovery = 41% Analysis Date = 07/05/14 Pct Recovery = 41% Analysis Date = 06/26/14 Pct Recovery = 41% Analysis Date = 06/26/14 Pct Recovery = 41% Analysis Date = 06/17/14 Pct Recovery = 41% Analysis Date = 06/17/14 Pct Recovery = 41% Analysis Date = 06/07/14 Pct Recovery = 41% Analysis Date = 06/07/14 Pct Recovery = 41% Analysis Date = 05/29/14 Pct Recovery = 41% Analysis Date = 05/29/14 Pct Recovery = 41% Analysis Date = 05/20/14 Pct Recovery = 42% Analysis Date = 05/20/14 Pct Recovery = 42% Analysis Date = 05/11/14 Pct Recovery = 42% Analysis Date = 05/11/14 Pct Recovery = 42% Analysis Date = 05/01/14 Pct Recovery = 42% Analysis Date = 05/01/14 Pct Recovery = 42% Analysis Date = 04/22/14 Pct Recovery = 42% Analysis Date = 04/22/14 Pct Recovery = 42% Analysis Date = 04/13/14 Pct Recovery = 42% Analysis Date = 04/13/14 Pct Recovery = 42% Analysis Date = 04/04/14 Pct Recovery = 42% Analysis Date = 04/04/14 Pct Recovery = 42% Analysis Date = 03/25/14 Pct Recovery = 42% Analysis Date = 03/25/14 Pct Recovery = 42% Analysis Date = 03/16/14 Pct Recovery = 42% Analysis Date = 03/16/14 Pct Recovery = 42% Analysis Date = 03/07/14 Pct Recovery = 42% Analysis Date = 03/07/14 Pct Recovery = 42% Analysis Date = 02/26/14 Pct Recovery = 43% Analysis Date = 02/26/14 Pct Recovery = 43% Analysis Date = 02/16/14 Pct Recovery = 43% Analysis Date = 02/16/14 Pct Recovery = 43% Analysis Date = 02/07/14 Pct Recovery = 43% Analysis Date = 02/07/14 Pct Recovery = 43% Analysis Date = 01/29/14 Pct Recovery = 43% Analysis Date = 01/29/14 Pct Recovery = 43% Analysis Date = 01/20/14 Pct Recovery = 43% Analysis Date = 01/20/14 Pct Recovery = 43% Analysis Date = 01/10/14 Pct Recovery = 43% Analysis Date = 01/10/14 Pct Recovery = 43% Analysis Date = 01/01/14 Pct Recovery = 43% Analysis Date = 01/01/14 Pct Recovery = 43% Analysis Date = 12/23/13 Pct Recovery = 43% Analysis Date = 12/23/13 Pct Recovery = 43% Analysis Date = 12/14/13 Pct Recovery = 43% Analysis Date = 12/14/13 Pct Recovery = 43% Analysis Date = 12/04/13 Pct Recovery = 43% Analysis Date = 12/04/13 Pct Recovery = 43% Analysis Date = 11/25/13 Pct Recovery = 43% Analysis Date = 11/25/13 Pct Recovery = 43% Analysis Date = 11/16/13 Pct Recovery = 43% Analysis Date = 11/16/13 Pct Recovery = 43% Analysis Date = 11/07/13 Pct Recovery = 43% Analysis Date = 11/07/13 Pct Recovery = 43% Analysis Date = 10/28/13 Pct Recovery = 43% Analysis Date = 10/28/13 Pct Recovery = 43% Analysis Date = 10/19/13 Pct Recovery = 44% Analysis Date = 10/19/13 Pct Recovery = 44% Analysis Date = 10/10/13 Pct Recovery = 44% Analysis Date = 10/10/13 Pct Recovery = 44% Analysis Date = 10/01/13 Pct Recovery = 44% Analysis Date = 10/01/13 Pct Recovery = 44% Analysis Date = 09/21/13 Pct Recovery = 44% Analysis Date = 09/21/13 Pct Recovery = 44% Analysis Date = 09/12/13 Pct Recovery = 44% Analysis Date = 09/12/13 Pct Recovery = 44% Analysis Date = 09/03/13 Pct Recovery = 44% Analysis Date = 09/03/13 Pct Recovery = 44% Analysis Date = 08/25/13 Pct Recovery = 44% Analysis Date = 08/25/13 Pct Recovery = 44% Analysis Date = 08/15/13 Pct Recovery = 44% Analysis Date = 08/15/13 Pct Recovery = 44% Analysis Date = 08/06/13 Pct Recovery = 44% Analysis Date = 08/06/13 Pct Recovery = 44% Analysis Date = 07/28/13 Pct Recovery = 44% Analysis Date = 07/28/13 Pct Recovery = 44% Analysis Date = 07/19/13 Pct Recovery = 44% Analysis Date = 07/19/13 Pct Recovery = 44% Analysis Date = 07/09/13 Pct Recovery = 44% Analysis Date = 07/09/13 Pct Recovery = 44% Analysis Date = 06/30/13 Pct Recovery = 44% Analysis Date = 06/30/13 Pct Recovery = 44% Analysis Date = 06/21/13 Pct Recovery = 44% Analysis Date = 06/21/13 Pct Recovery = 44% Analysis Date = 06/12/13 Pct Recovery = 44% Analysis Date = 06/12/13 Pct Recovery = 44% Analysis Date = 06/02/13 Pct Recovery = 44% Analysis Date = 06/02/13 Pct Recovery = 44% Analysis Date = 05/24/13 Pct Recovery = 45% Analysis Date = 05/24/13 Pct Recovery = 45% Analysis Date = 05/15/13 Pct Recovery = 45% Analysis Date = 05/15/13 Pct Recovery = 45% Analysis Date = 05/06/13 Pct Recovery = 45% Analysis Date = 05/06/13 Pct Recovery = 45% Analysis Date = 04/26/13 Pct Recovery = 45% Analysis Date = 04/26/13 Pct Recovery = 45% Analysis Date = 04/17/13 Pct Recovery = 45% Analysis Date = 04/17/13 Pct Recovery = 45% Analysis Date = 04/08/13 Pct Recovery = 45% Analysis Date = 04/08/13 Pct Recovery = 45% Analysis Date = 03/30/13 Pct Recovery = 45% Analysis Date = 03/30/13 Pct Recovery = 45% Analysis Date = 03/20/13 Pct Recovery = 45% Analysis Date = 03/20/13 Pct Recovery = 45% Analysis Date = 03/11/13 Pct Recovery = 45% Analysis Date = 03/11/13 Pct Recovery = 45% Analysis Date = 03/02/13 Pct Recovery = 45% Analysis Date = 03/02/13 Pct Recovery = 45% Analysis Date = 02/21/13 Pct Recovery = 45% Analysis Date = 02/21/13 Pct Recovery = 45% Analysis Date = 02/11/13 Pct Recovery = 45% Analysis Date = 02/11/13 Pct Recovery = 45% Analysis Date = 02/02/13 Pct Recovery = 45% Analysis Date = 02/02/13 Pct Recovery = 45% Analysis Date = 01/24/13 Pct Recovery = 45% Analysis Date = 01/24/13 Pct Recovery = 45% Analysis Date = 01/15/13 Pct Recovery = 45% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
DIMETHOATE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 65 40% 11% 38% 10%
Total 65 40% 11% 38% 10%

Sample Statistics
DIMETHOATE

Characteristic N % % Basis
Plotted 65 94% Spiked
Estimated Values 65 94% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 69 .  
False Negatives 4 6% 4 out of 69
Not Spiked 49 .  
False Positives 0 0% 0 out of 49

OBSP Determination:
DISULFOTON
METHOD: 2033 , TESTIDCODE: 82677GCM35

Laboratory ID = 20140100085 Lab Value = 0.405 Expected Conc. = 0.45 Report level label = 0.04 Pct Recovery = 90% Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl SpecificMix = T1130514013 Laboratory ID = 20132490342 Lab Value = 0.194 Expected Conc. = 0.45 Report level label = 0.04 Pct Recovery = 43% Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl SpecificMix = T1130514013 Laboratory ID = 20163370001 Lab Value = 0.193 Expected Conc. = 0.255 Report level label = 0.04 Pct Recovery = 76% Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl SpecificMix = B20160331 Laboratory ID = 20163150006 Lab Value = 0.178 Expected Conc. = 0.255 Report level label = 0.04 Pct Recovery = 70% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl SpecificMix = B20160331 Laboratory ID = 20161880109 Lab Value = 0.224 Expected Conc. = 0.247 Report level label = 0.04 Pct Recovery = 91% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl SpecificMix = 03FF076 Laboratory ID = 20130250061 Lab Value = 0.092 Expected Conc. = 0.247 Report level label = 0.04 Pct Recovery = 37% Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl SpecificMix = 05BB029 Laboratory ID = 20140370077 Lab Value = 0.173 Expected Conc. = 0.225 Report level label = 0.04 Pct Recovery = 77% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl SpecificMix = T1130514013 Laboratory ID = 20132690010 Lab Value = 0.144 Expected Conc. = 0.225 Report level label = 0.04 Pct Recovery = 64% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl SpecificMix = T1130514013 Laboratory ID = 20171720140 Lab Value = 0.189 Expected Conc. = 0.204 Report level label = 0.04 Pct Recovery = 93% Analysis Date = 08/31/17 SpikeMix = Supelco LC20138V: 80 µl & Phenova B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20171660002 Lab Value = 0.176 Expected Conc. = 0.204 Report level label = 0.04 Pct Recovery = 86% Analysis Date = 08/23/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20170190026 Lab Value = 0.163 Expected Conc. = 0.204 Report level label = 0.04 Pct Recovery = 80% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20161470001 Lab Value = 0.169 Expected Conc. = 0.204 Report level label = 0.04 Pct Recovery = 83% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20170960001 Lab Value = 0.134 Expected Conc. = 0.1976 Report level label = 0.04 Pct Recovery = 68% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl SpecificMix = 03FF076 Laboratory ID = 20150430092 Lab Value = 0.108 Expected Conc. = 0.162 Report level label = 0.04 Pct Recovery = 67% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl SpecificMix = E1140407002 Laboratory ID = 20143110108 Lab Value = 0.062 Expected Conc. = 0.162 Report level label = 0.04 Pct Recovery = 38% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl SpecificMix = E1140407002 Laboratory ID = 20142720002 Lab Value = 0.066 Expected Conc. = 0.162 Report level label = 0.04 Pct Recovery = 41% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl SpecificMix = E1140407002 Laboratory ID = 20141770149 Lab Value = 0.072 Expected Conc. = 0.162 Report level label = 0.04 Pct Recovery = 44% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl SpecificMix = E1140407002 Laboratory ID = 20143240095 Lab Value = 0.068 Expected Conc. = 0.1608 Report level label = 0.04 Pct Recovery = 42% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl SpecificMix = 032714 Laboratory ID = 20142270001 Lab Value = 0.049 Expected Conc. = 0.1608 Report level label = 0.04 Pct Recovery = 30% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl SpecificMix = 032714 Laboratory ID = 20141220025 Lab Value = 0.062 Expected Conc. = 0.1608 Report level label = 0.04 Pct Recovery = 39% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl SpecificMix = 032714 Laboratory ID = 20172230001 Lab Value = 0.085 Expected Conc. = 0.135 Report level label = 0.04 Pct Recovery = 63% Analysis Date = 10/19/17 SpikeMix = ChemService 6472100: 50 µl & Abs 071717Pest: 50 µl SpecificMix = 6472100 Laboratory ID = 20172560101 Lab Value = 0.063 Expected Conc. = 0.1345 Report level label = 0.04 Pct Recovery = 47% Analysis Date = 12/22/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6567600: 50 µl SpecificMix = EN170808006 Laboratory ID = 20172370001 Lab Value = 0.067 Expected Conc. = 0.1345 Report level label = 0.04 Pct Recovery = 50% Analysis Date = 11/18/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6537100: 50 µl SpecificMix = EN170808006 Laboratory ID = 20140230082 Lab Value = 0.085 Expected Conc. = 0.126 Report level label = 0.04 Pct Recovery = 67% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl SpecificMix = 012513 Laboratory ID = 20132420001 Lab Value = 0.038 Expected Conc. = 0.126 Report level label = 0.04 Pct Recovery = 30% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl SpecificMix = 012513 Laboratory ID = 20130100066 Lab Value = 0.022 Expected Conc. = 0.125 Report level label = 0.04 Pct Recovery = 18% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl SpecificMix = 052412 Laboratory ID = 20161260151 Lab Value = 0.075 Expected Conc. = 0.12 Report level label = 0.04 Pct Recovery = 63% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = EN150513008 Laboratory ID = 20160770090 Lab Value = 0.050 Expected Conc. = 0.12 Report level label = 0.04 Pct Recovery = 42% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = EN150513008 Laboratory ID = 20153510109 Lab Value = 0.065 Expected Conc. = 0.12 Report level label = 0.04 Pct Recovery = 54% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = EN150513008 Laboratory ID = 20171160110 Lab Value = 0.061 Expected Conc. = 0.102 Report level label = 0.04 Pct Recovery = 60% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = B20160331 Laboratory ID = 20162380004 Lab Value = 0.066 Expected Conc. = 0.102 Report level label = 0.04 Pct Recovery = 65% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = B20160331 Laboratory ID = 20162150213 Lab Value = 0.067 Expected Conc. = 0.102 Report level label = 0.04 Pct Recovery = 66% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl SpecificMix = B20160331 Laboratory ID = 20172020035 Lab Value = 0.059 Expected Conc. = 0.0988 Report level label = 0.04 Pct Recovery = 60% Analysis Date = 11/07/17 SpikeMix = Abs 071717Pest: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20171510080 Lab Value = 0.072 Expected Conc. = 0.0988 Report level label = 0.04 Pct Recovery = 73% Analysis Date = 06/09/17 SpikeMix = Supelco LC20138V: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20170460061 Lab Value = 0.059 Expected Conc. = 0.0988 Report level label = 0.04 Pct Recovery = 60% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl SpecificMix = 03FF076 Laboratory ID = 20162660005 Lab Value = 0.043 Expected Conc. = 0.0988 Report level label = 0.04 Pct Recovery = 44% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl SpecificMix = 03FF076 Laboratory ID = 20161600087 Lab Value = 0.057 Expected Conc. = 0.0988 Report level label = 0.04 Pct Recovery = 58% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20161340228 Lab Value = 0.059 Expected Conc. = 0.0988 Report level label = 0.04 Pct Recovery = 60% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl SpecificMix = 03FF076 Laboratory ID = 20161190075 Lab Value = 0.047 Expected Conc. = 0.0988 Report level label = 0.04 Pct Recovery = 48% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20140730138 Lab Value = 0.049 Expected Conc. = 0.0904 Report level label = 0.04 Pct Recovery = 54% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 1473000 Laboratory ID = 20133470008 Lab Value = 0.006 Expected Conc. = 0.0904 Report level label = 0.04 Pct Recovery = 7% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl SpecificMix = 1473000 Laboratory ID = 20133310030 Lab Value = 0.057 Expected Conc. = 0.0904 Report level label = 0.04 Pct Recovery = 63% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl SpecificMix = 1473000 Laboratory ID = 20133050050 Lab Value = 0.045 Expected Conc. = 0.09 Report level label = 0.04 Pct Recovery = 50% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl SpecificMix = T1130514013 Laboratory ID = 20173120093 Lab Value = 0.028 Expected Conc. = 0.081 Report level label = 0.04 Pct Recovery = 35% Analysis Date = 03/10/18 SpikeMix = ChemService 6472100: 30 µl & ChemService 6537100: 30 µl SpecificMix = 6472100 Laboratory ID = 20142470041 Lab Value = 0.006 Expected Conc. = 0.081 Report level label = 0.04 Pct Recovery = 7% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141910243 Lab Value = 0.018 Expected Conc. = 0.081 Report level label = 0.04 Pct Recovery = 22% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141640076 Lab Value = 0.021 Expected Conc. = 0.081 Report level label = 0.04 Pct Recovery = 26% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141360094 Lab Value = 0.024 Expected Conc. = 0.081 Report level label = 0.04 Pct Recovery = 30% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = E1140407002 Laboratory ID = 20150150115 Lab Value = 0.019 Expected Conc. = 0.0804 Report level label = 0.04 Pct Recovery = 24% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl SpecificMix = 032714 Laboratory ID = 20142820151 Lab Value = 0.005 Expected Conc. = 0.0804 Report level label = 0.04 Pct Recovery = 6% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl SpecificMix = 032714 Laboratory ID = 20141490205 Lab Value = 0.049 Expected Conc. = 0.0804 Report level label = 0.04 Pct Recovery = 61% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = 032714 Laboratory ID = 20141080004 Lab Value = 0.030 Expected Conc. = 0.0804 Report level label = 0.04 Pct Recovery = 37% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl SpecificMix = 032714 Laboratory ID = 20161050143 Lab Value = 0.031 Expected Conc. = 0.0602 Report level label = 0.04 Pct Recovery = 51% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Laboratory ID = 20160430111 Lab Value = 0.024 Expected Conc. = 0.0602 Report level label = 0.04 Pct Recovery = 40% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Laboratory ID = 20160070059 Lab Value = 0.036 Expected Conc. = 0.0602 Report level label = 0.04 Pct Recovery = 60% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = 040615 Laboratory ID = 20151380009 Lab Value = 0.004 Expected Conc. = 0.0602 Report level label = 0.04 Pct Recovery = 7% Analysis Date = 05/30/15 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Laboratory ID = 20151210037 Lab Value = 0.009 Expected Conc. = 0.0602 Report level label = 0.04 Pct Recovery = 15% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Laboratory ID = 20160560044 Lab Value = 0.019 Expected Conc. = 0.06 Report level label = 0.04 Pct Recovery = 32% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl SpecificMix = EN150513008 Laboratory ID = 20153160001 Lab Value = 0.012 Expected Conc. = 0.06 Report level label = 0.04 Pct Recovery = 20% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = EN150513008 Laboratory ID = 20153030068 Lab Value = 0.031 Expected Conc. = 0.06 Report level label = 0.04 Pct Recovery = 52% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150513008 Laboratory ID = 20140860102 Lab Value = 0.015 Expected Conc. = 0.0504 Report level label = 0.04 Pct Recovery = 30% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 012513 Laboratory ID = 20131920149 Lab Value = 0.006 Expected Conc. = 0.0504 Report level label = 0.04 Pct Recovery = 12% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl SpecificMix = 012513 Laboratory ID = 20133400002 Lab Value = 0.024 Expected Conc. = 0.05 Report level label = 0.04 Pct Recovery = 48% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = 052412 Laboratory ID = 20132910008 Lab Value = 0.029 Expected Conc. = 0.05 Report level label = 0.04 Pct Recovery = 58% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = 052412 Laboratory ID = 20130650005 Lab Value = 0.004 Expected Conc. = 0.05 Report level label = 0.04 Pct Recovery = 8% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl SpecificMix = 052412 Analysis Date = 03/09/18 Pct Recovery = 67% Analysis Date = 02/28/18 Pct Recovery = 67% Analysis Date = 02/28/18 Pct Recovery = 67% Analysis Date = 02/19/18 Pct Recovery = 67% Analysis Date = 02/19/18 Pct Recovery = 67% Analysis Date = 02/09/18 Pct Recovery = 67% Analysis Date = 02/09/18 Pct Recovery = 67% Analysis Date = 01/31/18 Pct Recovery = 67% Analysis Date = 01/31/18 Pct Recovery = 67% Analysis Date = 01/22/18 Pct Recovery = 67% Analysis Date = 01/22/18 Pct Recovery = 67% Analysis Date = 01/12/18 Pct Recovery = 67% Analysis Date = 01/12/18 Pct Recovery = 67% Analysis Date = 01/03/18 Pct Recovery = 67% Analysis Date = 01/03/18 Pct Recovery = 67% Analysis Date = 12/24/17 Pct Recovery = 66% Analysis Date = 12/24/17 Pct Recovery = 66% Analysis Date = 12/15/17 Pct Recovery = 66% Analysis Date = 12/15/17 Pct Recovery = 66% Analysis Date = 12/06/17 Pct Recovery = 66% Analysis Date = 12/06/17 Pct Recovery = 66% Analysis Date = 11/26/17 Pct Recovery = 66% Analysis Date = 11/26/17 Pct Recovery = 66% Analysis Date = 11/17/17 Pct Recovery = 66% Analysis Date = 11/17/17 Pct Recovery = 66% Analysis Date = 11/07/17 Pct Recovery = 66% Analysis Date = 11/07/17 Pct Recovery = 66% Analysis Date = 10/29/17 Pct Recovery = 66% Analysis Date = 10/29/17 Pct Recovery = 66% Analysis Date = 10/20/17 Pct Recovery = 66% Analysis Date = 10/20/17 Pct Recovery = 66% Analysis Date = 10/10/17 Pct Recovery = 66% Analysis Date = 10/10/17 Pct Recovery = 66% Analysis Date = 10/01/17 Pct Recovery = 65% Analysis Date = 10/01/17 Pct Recovery = 65% Analysis Date = 09/21/17 Pct Recovery = 65% Analysis Date = 09/21/17 Pct Recovery = 65% Analysis Date = 09/12/17 Pct Recovery = 65% Analysis Date = 09/12/17 Pct Recovery = 65% Analysis Date = 09/03/17 Pct Recovery = 65% Analysis Date = 09/03/17 Pct Recovery = 65% Analysis Date = 08/24/17 Pct Recovery = 65% Analysis Date = 08/24/17 Pct Recovery = 65% Analysis Date = 08/15/17 Pct Recovery = 65% Analysis Date = 08/15/17 Pct Recovery = 65% Analysis Date = 08/06/17 Pct Recovery = 64% Analysis Date = 08/06/17 Pct Recovery = 64% Analysis Date = 07/27/17 Pct Recovery = 64% Analysis Date = 07/27/17 Pct Recovery = 64% Analysis Date = 07/18/17 Pct Recovery = 64% Analysis Date = 07/18/17 Pct Recovery = 64% Analysis Date = 07/08/17 Pct Recovery = 64% Analysis Date = 07/08/17 Pct Recovery = 64% Analysis Date = 06/29/17 Pct Recovery = 64% Analysis Date = 06/29/17 Pct Recovery = 64% Analysis Date = 06/20/17 Pct Recovery = 64% Analysis Date = 06/20/17 Pct Recovery = 64% Analysis Date = 06/10/17 Pct Recovery = 64% Analysis Date = 06/10/17 Pct Recovery = 64% Analysis Date = 06/01/17 Pct Recovery = 63% Analysis Date = 06/01/17 Pct Recovery = 63% Analysis Date = 05/22/17 Pct Recovery = 63% Analysis Date = 05/22/17 Pct Recovery = 63% Analysis Date = 05/13/17 Pct Recovery = 63% Analysis Date = 05/13/17 Pct Recovery = 63% Analysis Date = 05/04/17 Pct Recovery = 63% Analysis Date = 05/04/17 Pct Recovery = 63% Analysis Date = 04/24/17 Pct Recovery = 63% Analysis Date = 04/24/17 Pct Recovery = 63% Analysis Date = 04/15/17 Pct Recovery = 63% Analysis Date = 04/15/17 Pct Recovery = 63% Analysis Date = 04/05/17 Pct Recovery = 62% Analysis Date = 04/05/17 Pct Recovery = 62% Analysis Date = 03/27/17 Pct Recovery = 62% Analysis Date = 03/27/17 Pct Recovery = 62% Analysis Date = 03/18/17 Pct Recovery = 62% Analysis Date = 03/18/17 Pct Recovery = 62% Analysis Date = 03/08/17 Pct Recovery = 62% Analysis Date = 03/08/17 Pct Recovery = 62% Analysis Date = 02/27/17 Pct Recovery = 62% Analysis Date = 02/27/17 Pct Recovery = 62% Analysis Date = 02/18/17 Pct Recovery = 62% Analysis Date = 02/18/17 Pct Recovery = 62% Analysis Date = 02/08/17 Pct Recovery = 61% Analysis Date = 02/08/17 Pct Recovery = 61% Analysis Date = 01/30/17 Pct Recovery = 61% Analysis Date = 01/30/17 Pct Recovery = 61% Analysis Date = 01/20/17 Pct Recovery = 61% Analysis Date = 01/20/17 Pct Recovery = 61% Analysis Date = 01/11/17 Pct Recovery = 61% Analysis Date = 01/11/17 Pct Recovery = 61% Analysis Date = 01/02/17 Pct Recovery = 60% Analysis Date = 01/02/17 Pct Recovery = 60% Analysis Date = 12/23/16 Pct Recovery = 60% Analysis Date = 12/23/16 Pct Recovery = 60% Analysis Date = 12/14/16 Pct Recovery = 60% Analysis Date = 12/14/16 Pct Recovery = 60% Analysis Date = 12/04/16 Pct Recovery = 60% Analysis Date = 12/04/16 Pct Recovery = 60% Analysis Date = 11/25/16 Pct Recovery = 59% Analysis Date = 11/25/16 Pct Recovery = 59% Analysis Date = 11/16/16 Pct Recovery = 59% Analysis Date = 11/16/16 Pct Recovery = 59% Analysis Date = 11/06/16 Pct Recovery = 59% Analysis Date = 11/06/16 Pct Recovery = 59% Analysis Date = 10/28/16 Pct Recovery = 59% Analysis Date = 10/28/16 Pct Recovery = 59% Analysis Date = 10/18/16 Pct Recovery = 59% Analysis Date = 10/18/16 Pct Recovery = 59% Analysis Date = 10/09/16 Pct Recovery = 58% Analysis Date = 10/09/16 Pct Recovery = 58% Analysis Date = 09/30/16 Pct Recovery = 58% Analysis Date = 09/30/16 Pct Recovery = 58% Analysis Date = 09/20/16 Pct Recovery = 58% Analysis Date = 09/20/16 Pct Recovery = 58% Analysis Date = 09/11/16 Pct Recovery = 57% Analysis Date = 09/11/16 Pct Recovery = 57% Analysis Date = 09/01/16 Pct Recovery = 57% Analysis Date = 09/01/16 Pct Recovery = 57% Analysis Date = 08/23/16 Pct Recovery = 57% Analysis Date = 08/23/16 Pct Recovery = 57% Analysis Date = 08/14/16 Pct Recovery = 56% Analysis Date = 08/14/16 Pct Recovery = 56% Analysis Date = 08/04/16 Pct Recovery = 56% Analysis Date = 08/04/16 Pct Recovery = 56% Analysis Date = 07/26/16 Pct Recovery = 55% Analysis Date = 07/26/16 Pct Recovery = 55% Analysis Date = 07/17/16 Pct Recovery = 55% Analysis Date = 07/17/16 Pct Recovery = 55% Analysis Date = 07/07/16 Pct Recovery = 55% Analysis Date = 07/07/16 Pct Recovery = 55% Analysis Date = 06/28/16 Pct Recovery = 54% Analysis Date = 06/28/16 Pct Recovery = 54% Analysis Date = 06/18/16 Pct Recovery = 54% Analysis Date = 06/18/16 Pct Recovery = 54% Analysis Date = 06/09/16 Pct Recovery = 53% Analysis Date = 06/09/16 Pct Recovery = 53% Analysis Date = 05/31/16 Pct Recovery = 53% Analysis Date = 05/31/16 Pct Recovery = 53% Analysis Date = 05/21/16 Pct Recovery = 52% Analysis Date = 05/21/16 Pct Recovery = 52% Analysis Date = 05/12/16 Pct Recovery = 52% Analysis Date = 05/12/16 Pct Recovery = 52% Analysis Date = 05/02/16 Pct Recovery = 51% Analysis Date = 05/02/16 Pct Recovery = 51% Analysis Date = 04/23/16 Pct Recovery = 51% Analysis Date = 04/23/16 Pct Recovery = 51% Analysis Date = 04/14/16 Pct Recovery = 50% Analysis Date = 04/14/16 Pct Recovery = 50% Analysis Date = 04/04/16 Pct Recovery = 50% Analysis Date = 04/04/16 Pct Recovery = 50% Analysis Date = 03/26/16 Pct Recovery = 49% Analysis Date = 03/26/16 Pct Recovery = 49% Analysis Date = 03/16/16 Pct Recovery = 49% Analysis Date = 03/16/16 Pct Recovery = 49% Analysis Date = 03/07/16 Pct Recovery = 48% Analysis Date = 03/07/16 Pct Recovery = 48% Analysis Date = 02/27/16 Pct Recovery = 48% Analysis Date = 02/27/16 Pct Recovery = 48% Analysis Date = 02/17/16 Pct Recovery = 48% Analysis Date = 02/17/16 Pct Recovery = 48% Analysis Date = 02/08/16 Pct Recovery = 47% Analysis Date = 02/08/16 Pct Recovery = 47% Analysis Date = 01/30/16 Pct Recovery = 47% Analysis Date = 01/30/16 Pct Recovery = 47% Analysis Date = 01/20/16 Pct Recovery = 46% Analysis Date = 01/20/16 Pct Recovery = 46% Analysis Date = 01/11/16 Pct Recovery = 46% Analysis Date = 01/11/16 Pct Recovery = 46% Analysis Date = 01/01/16 Pct Recovery = 45% Analysis Date = 01/01/16 Pct Recovery = 45% Analysis Date = 12/23/15 Pct Recovery = 45% Analysis Date = 12/23/15 Pct Recovery = 45% Analysis Date = 12/14/15 Pct Recovery = 45% Analysis Date = 12/14/15 Pct Recovery = 45% Analysis Date = 12/04/15 Pct Recovery = 44% Analysis Date = 12/04/15 Pct Recovery = 44% Analysis Date = 11/25/15 Pct Recovery = 44% Analysis Date = 11/25/15 Pct Recovery = 44% Analysis Date = 11/15/15 Pct Recovery = 43% Analysis Date = 11/15/15 Pct Recovery = 43% Analysis Date = 11/06/15 Pct Recovery = 43% Analysis Date = 11/06/15 Pct Recovery = 43% Analysis Date = 10/28/15 Pct Recovery = 43% Analysis Date = 10/28/15 Pct Recovery = 43% Analysis Date = 10/18/15 Pct Recovery = 42% Analysis Date = 10/18/15 Pct Recovery = 42% Analysis Date = 10/09/15 Pct Recovery = 42% Analysis Date = 10/09/15 Pct Recovery = 42% Analysis Date = 09/29/15 Pct Recovery = 41% Analysis Date = 09/29/15 Pct Recovery = 41% Analysis Date = 09/20/15 Pct Recovery = 41% Analysis Date = 09/20/15 Pct Recovery = 41% Analysis Date = 09/11/15 Pct Recovery = 41% Analysis Date = 09/11/15 Pct Recovery = 41% Analysis Date = 09/01/15 Pct Recovery = 40% Analysis Date = 09/01/15 Pct Recovery = 40% Analysis Date = 08/23/15 Pct Recovery = 40% Analysis Date = 08/23/15 Pct Recovery = 40% Analysis Date = 08/13/15 Pct Recovery = 39% Analysis Date = 08/13/15 Pct Recovery = 39% Analysis Date = 08/04/15 Pct Recovery = 39% Analysis Date = 08/04/15 Pct Recovery = 39% Analysis Date = 07/26/15 Pct Recovery = 39% Analysis Date = 07/26/15 Pct Recovery = 39% Analysis Date = 07/16/15 Pct Recovery = 38% Analysis Date = 07/16/15 Pct Recovery = 38% Analysis Date = 07/07/15 Pct Recovery = 38% Analysis Date = 07/07/15 Pct Recovery = 38% Analysis Date = 06/28/15 Pct Recovery = 37% Analysis Date = 06/28/15 Pct Recovery = 37% Analysis Date = 06/18/15 Pct Recovery = 37% Analysis Date = 06/18/15 Pct Recovery = 37% Analysis Date = 06/09/15 Pct Recovery = 37% Analysis Date = 06/09/15 Pct Recovery = 37% Analysis Date = 05/30/15 Pct Recovery = 36% Analysis Date = 05/30/15 Pct Recovery = 36% Analysis Date = 05/21/15 Pct Recovery = 36% Analysis Date = 05/21/15 Pct Recovery = 36% Analysis Date = 05/12/15 Pct Recovery = 35% Analysis Date = 05/12/15 Pct Recovery = 35% Analysis Date = 05/02/15 Pct Recovery = 35% Analysis Date = 05/02/15 Pct Recovery = 35% Analysis Date = 04/23/15 Pct Recovery = 35% Analysis Date = 04/23/15 Pct Recovery = 35% Analysis Date = 04/13/15 Pct Recovery = 35% Analysis Date = 04/13/15 Pct Recovery = 35% Analysis Date = 04/04/15 Pct Recovery = 35% Analysis Date = 04/04/15 Pct Recovery = 35% Analysis Date = 03/26/15 Pct Recovery = 35% Analysis Date = 03/26/15 Pct Recovery = 35% Analysis Date = 03/16/15 Pct Recovery = 34% Analysis Date = 03/16/15 Pct Recovery = 34% Analysis Date = 03/07/15 Pct Recovery = 34% Analysis Date = 03/07/15 Pct Recovery = 34% Analysis Date = 02/25/15 Pct Recovery = 34% Analysis Date = 02/25/15 Pct Recovery = 34% Analysis Date = 02/16/15 Pct Recovery = 34% Analysis Date = 02/16/15 Pct Recovery = 34% Analysis Date = 02/07/15 Pct Recovery = 34% Analysis Date = 02/07/15 Pct Recovery = 34% Analysis Date = 01/28/15 Pct Recovery = 34% Analysis Date = 01/28/15 Pct Recovery = 34% Analysis Date = 01/19/15 Pct Recovery = 33% Analysis Date = 01/19/15 Pct Recovery = 33% Analysis Date = 01/10/15 Pct Recovery = 33% Analysis Date = 01/10/15 Pct Recovery = 33% Analysis Date = 12/31/14 Pct Recovery = 33% Analysis Date = 12/31/14 Pct Recovery = 33% Analysis Date = 12/22/14 Pct Recovery = 33% Analysis Date = 12/22/14 Pct Recovery = 33% Analysis Date = 12/12/14 Pct Recovery = 33% Analysis Date = 12/12/14 Pct Recovery = 33% Analysis Date = 12/03/14 Pct Recovery = 33% Analysis Date = 12/03/14 Pct Recovery = 33% Analysis Date = 11/24/14 Pct Recovery = 32% Analysis Date = 11/24/14 Pct Recovery = 32% Analysis Date = 11/14/14 Pct Recovery = 32% Analysis Date = 11/14/14 Pct Recovery = 32% Analysis Date = 11/05/14 Pct Recovery = 33% Analysis Date = 11/05/14 Pct Recovery = 33% Analysis Date = 10/26/14 Pct Recovery = 33% Analysis Date = 10/26/14 Pct Recovery = 33% Analysis Date = 10/17/14 Pct Recovery = 34% Analysis Date = 10/17/14 Pct Recovery = 34% Analysis Date = 10/08/14 Pct Recovery = 34% Analysis Date = 10/08/14 Pct Recovery = 34% Analysis Date = 09/28/14 Pct Recovery = 35% Analysis Date = 09/28/14 Pct Recovery = 35% Analysis Date = 09/19/14 Pct Recovery = 35% Analysis Date = 09/19/14 Pct Recovery = 35% Analysis Date = 09/09/14 Pct Recovery = 35% Analysis Date = 09/09/14 Pct Recovery = 35% Analysis Date = 08/31/14 Pct Recovery = 36% Analysis Date = 08/31/14 Pct Recovery = 36% Analysis Date = 08/22/14 Pct Recovery = 36% Analysis Date = 08/22/14 Pct Recovery = 36% Analysis Date = 08/12/14 Pct Recovery = 37% Analysis Date = 08/12/14 Pct Recovery = 37% Analysis Date = 08/03/14 Pct Recovery = 37% Analysis Date = 08/03/14 Pct Recovery = 37% Analysis Date = 07/25/14 Pct Recovery = 37% Analysis Date = 07/25/14 Pct Recovery = 37% Analysis Date = 07/15/14 Pct Recovery = 38% Analysis Date = 07/15/14 Pct Recovery = 38% Analysis Date = 07/06/14 Pct Recovery = 38% Analysis Date = 07/06/14 Pct Recovery = 38% Analysis Date = 06/26/14 Pct Recovery = 39% Analysis Date = 06/26/14 Pct Recovery = 39% Analysis Date = 06/17/14 Pct Recovery = 39% Analysis Date = 06/17/14 Pct Recovery = 39% Analysis Date = 06/08/14 Pct Recovery = 39% Analysis Date = 06/08/14 Pct Recovery = 39% Analysis Date = 05/29/14 Pct Recovery = 39% Analysis Date = 05/29/14 Pct Recovery = 39% Analysis Date = 05/20/14 Pct Recovery = 39% Analysis Date = 05/20/14 Pct Recovery = 39% Analysis Date = 05/10/14 Pct Recovery = 39% Analysis Date = 05/10/14 Pct Recovery = 39% Analysis Date = 05/01/14 Pct Recovery = 39% Analysis Date = 05/01/14 Pct Recovery = 39% Analysis Date = 04/22/14 Pct Recovery = 40% Analysis Date = 04/22/14 Pct Recovery = 40% Analysis Date = 04/12/14 Pct Recovery = 40% Analysis Date = 04/12/14 Pct Recovery = 40% Analysis Date = 04/03/14 Pct Recovery = 40% Analysis Date = 04/03/14 Pct Recovery = 40% Analysis Date = 03/24/14 Pct Recovery = 40% Analysis Date = 03/24/14 Pct Recovery = 40% Analysis Date = 03/15/14 Pct Recovery = 40% Analysis Date = 03/15/14 Pct Recovery = 40% Analysis Date = 03/06/14 Pct Recovery = 40% Analysis Date = 03/06/14 Pct Recovery = 40% Analysis Date = 02/24/14 Pct Recovery = 40% Analysis Date = 02/24/14 Pct Recovery = 40% Analysis Date = 02/15/14 Pct Recovery = 40% Analysis Date = 02/15/14 Pct Recovery = 40% Analysis Date = 02/05/14 Pct Recovery = 40% Analysis Date = 02/05/14 Pct Recovery = 40% Analysis Date = 01/27/14 Pct Recovery = 40% Analysis Date = 01/27/14 Pct Recovery = 40% Analysis Date = 01/18/14 Pct Recovery = 40% Analysis Date = 01/18/14 Pct Recovery = 40% Analysis Date = 01/08/14 Pct Recovery = 40% Analysis Date = 01/08/14 Pct Recovery = 40% Analysis Date = 12/30/13 Pct Recovery = 40% Analysis Date = 12/30/13 Pct Recovery = 40% Analysis Date = 12/21/13 Pct Recovery = 40% Analysis Date = 12/21/13 Pct Recovery = 40% Analysis Date = 12/11/13 Pct Recovery = 40% Analysis Date = 12/11/13 Pct Recovery = 40% Analysis Date = 12/02/13 Pct Recovery = 40% Analysis Date = 12/02/13 Pct Recovery = 40% Analysis Date = 11/22/13 Pct Recovery = 40% Analysis Date = 11/22/13 Pct Recovery = 40% Analysis Date = 11/13/13 Pct Recovery = 40% Analysis Date = 11/13/13 Pct Recovery = 40% Analysis Date = 11/04/13 Pct Recovery = 40% Analysis Date = 11/04/13 Pct Recovery = 40% Analysis Date = 10/25/13 Pct Recovery = 40% Analysis Date = 10/25/13 Pct Recovery = 40% Analysis Date = 10/16/13 Pct Recovery = 40% Analysis Date = 10/16/13 Pct Recovery = 40% Analysis Date = 10/06/13 Pct Recovery = 40% Analysis Date = 10/06/13 Pct Recovery = 40% Analysis Date = 09/27/13 Pct Recovery = 40% Analysis Date = 09/27/13 Pct Recovery = 40% Analysis Date = 09/18/13 Pct Recovery = 40% Analysis Date = 09/18/13 Pct Recovery = 40% Analysis Date = 09/08/13 Pct Recovery = 40% Analysis Date = 09/08/13 Pct Recovery = 40% Analysis Date = 08/30/13 Pct Recovery = 40% Analysis Date = 08/30/13 Pct Recovery = 40% Analysis Date = 08/20/13 Pct Recovery = 40% Analysis Date = 08/20/13 Pct Recovery = 40% Analysis Date = 08/11/13 Pct Recovery = 40% Analysis Date = 08/11/13 Pct Recovery = 40% Analysis Date = 08/02/13 Pct Recovery = 40% Analysis Date = 08/02/13 Pct Recovery = 40% Analysis Date = 07/23/13 Pct Recovery = 40% Analysis Date = 07/23/13 Pct Recovery = 40% Analysis Date = 07/14/13 Pct Recovery = 40% Analysis Date = 07/14/13 Pct Recovery = 40% Analysis Date = 07/05/13 Pct Recovery = 40% Analysis Date = 07/05/13 Pct Recovery = 40% Analysis Date = 06/25/13 Pct Recovery = 40% Analysis Date = 06/25/13 Pct Recovery = 40% Analysis Date = 06/16/13 Pct Recovery = 40% Analysis Date = 06/16/13 Pct Recovery = 40% Analysis Date = 06/06/13 Pct Recovery = 40% Analysis Date = 06/06/13 Pct Recovery = 40% Analysis Date = 05/28/13 Pct Recovery = 40% Analysis Date = 05/28/13 Pct Recovery = 40% Analysis Date = 05/19/13 Pct Recovery = 39% Analysis Date = 05/19/13 Pct Recovery = 39% Analysis Date = 05/09/13 Pct Recovery = 39% Analysis Date = 05/09/13 Pct Recovery = 39% Analysis Date = 04/30/13 Pct Recovery = 39% Analysis Date = 04/30/13 Pct Recovery = 39% Analysis Date = 04/20/13 Pct Recovery = 39% Analysis Date = 04/20/13 Pct Recovery = 39% Analysis Date = 04/11/13 Pct Recovery = 39% Analysis Date = 04/11/13 Pct Recovery = 39% Analysis Date = 04/02/13 Pct Recovery = 39% Analysis Date = 04/02/13 Pct Recovery = 39% Analysis Date = 03/23/13 Pct Recovery = 39% Analysis Date = 03/23/13 Pct Recovery = 39% Analysis Date = 03/14/13 Pct Recovery = 39% Analysis Date = 03/14/13 Pct Recovery = 39% Analysis Date = 03/04/13 Pct Recovery = 39% Analysis Date = 03/04/13 Pct Recovery = 39% Analysis Date = 02/23/13 Pct Recovery = 39% Analysis Date = 02/23/13 Pct Recovery = 39% Analysis Date = 02/14/13 Pct Recovery = 39% Analysis Date = 02/14/13 Pct Recovery = 39% Analysis Date = 02/04/13 Pct Recovery = 39% Analysis Date = 02/04/13 Pct Recovery = 39% Analysis Date = 01/26/13 Pct Recovery = 39% Analysis Date = 01/26/13 Pct Recovery = 39% Analysis Date = 01/17/13 Pct Recovery = 39% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
DISULFOTON

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 65 48% 23% 50% 23%
Total 65 48% 23% 50% 23%

Sample Statistics
DISULFOTON

Characteristic N % % Basis
Plotted 65 87% Spiked
Estimated Values 65 87% Spiked
Deleted Values 5 4% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 79 .  
False Negatives 10 13% 10 out of 75
Not Spiked 39 .  
False Positives 0 0% 0 out of 38

OBSP Determination:
DISULFOTON SULFONE
METHOD: 2033 , TESTIDCODE: 61640GCM39

Laboratory ID = 20152190003 Lab Value = 0.048 Expected Conc. = 0.0152 Report level label = 0.01 Pct Recovery = 314% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = 0406-15-01 Laboratory ID = 20130940097 Lab Value = 0.168 Expected Conc. = 0.2535 Report level label = 0.01 Pct Recovery = 66% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = 0507-12-04.2 Laboratory ID = 20123560092 Lab Value = 0.174 Expected Conc. = 0.2535 Report level label = 0.01 Pct Recovery = 69% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = 0507-12-04.2 Laboratory ID = 20130810108 Lab Value = 0.212 Expected Conc. = 0.25 Report level label = 0.01 Pct Recovery = 85% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl SpecificMix = LB92783 Laboratory ID = 20130100066 Lab Value = 0.182 Expected Conc. = 0.25 Report level label = 0.01 Pct Recovery = 73% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl SpecificMix = LB92783 Laboratory ID = 20130510051 Lab Value = 0.082 Expected Conc. = 0.1014 Report level label = 0.01 Pct Recovery = 81% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl SpecificMix = 0507-12-04.2 Laboratory ID = 20130390105 Lab Value = 0.075 Expected Conc. = 0.1 Report level label = 0.01 Pct Recovery = 75% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl SpecificMix = LB92783 Laboratory ID = 20162860079 Lab Value = 0.064 Expected Conc. = 0.063 Report level label = 0.01 Pct Recovery = 101% Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl SpecificMix = 060916 Laboratory ID = 20163150006 Lab Value = 0.058 Expected Conc. = 0.063 Report level label = 0.01 Pct Recovery = 93% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl SpecificMix = 060916 Laboratory ID = 20152610011 Lab Value = 0.100 Expected Conc. = 0.0606 Report level label = 0.01 Pct Recovery = 165% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl SpecificMix = 0406-15-01 Laboratory ID = 20152460215 Lab Value = 0.048 Expected Conc. = 0.0606 Report level label = 0.01 Pct Recovery = 78% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl SpecificMix = 0406-15-01 Laboratory ID = 20171660002 Lab Value = 0.049 Expected Conc. = 0.0504 Report level label = 0.01 Pct Recovery = 97% Analysis Date = 08/23/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = 060916 Laboratory ID = 20171380001 Lab Value = 0.043 Expected Conc. = 0.0504 Report level label = 0.01 Pct Recovery = 86% Analysis Date = 06/07/17 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 041816 Laboratory ID = 20170740063 Lab Value = 0.043 Expected Conc. = 0.0504 Report level label = 0.01 Pct Recovery = 84% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl SpecificMix = 041816 Laboratory ID = 20170190026 Lab Value = 0.050 Expected Conc. = 0.0504 Report level label = 0.01 Pct Recovery = 99% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = 060916 Laboratory ID = 20161740258 Lab Value = 0.035 Expected Conc. = 0.0504 Report level label = 0.01 Pct Recovery = 69% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 041816 Laboratory ID = 20143240095 Lab Value = 0.043 Expected Conc. = 0.0402 Report level label = 0.01 Pct Recovery = 106% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl SpecificMix = 032714 Laboratory ID = 20142270001 Lab Value = 0.045 Expected Conc. = 0.0402 Report level label = 0.01 Pct Recovery = 111% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl SpecificMix = 032714 Laboratory ID = 20141220025 Lab Value = 0.044 Expected Conc. = 0.0402 Report level label = 0.01 Pct Recovery = 108% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl SpecificMix = 032714 Laboratory ID = 20150430092 Lab Value = 0.038 Expected Conc. = 0.0401 Report level label = 0.01 Pct Recovery = 94% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl SpecificMix = E1140407002 Laboratory ID = 20143110108 Lab Value = 0.038 Expected Conc. = 0.0401 Report level label = 0.01 Pct Recovery = 94% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl SpecificMix = E1140407002 Laboratory ID = 20142720002 Lab Value = 0.042 Expected Conc. = 0.0401 Report level label = 0.01 Pct Recovery = 105% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl SpecificMix = E1140407002 Laboratory ID = 20141770149 Lab Value = 0.034 Expected Conc. = 0.0401 Report level label = 0.01 Pct Recovery = 85% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl SpecificMix = E1140407002 Laboratory ID = 20172230001 Lab Value = 0.035 Expected Conc. = 0.035 Report level label = 0.01 Pct Recovery = 101% Analysis Date = 10/19/17 SpikeMix = ChemService 6472100: 50 µl & Abs 071717Pest: 50 µl SpecificMix = 6472100 Laboratory ID = 20172560101 Lab Value = 0.036 Expected Conc. = 0.0338 Report level label = 0.01 Pct Recovery = 107% Analysis Date = 12/22/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6567600: 50 µl SpecificMix = EN170808006 Laboratory ID = 20172370001 Lab Value = 0.044 Expected Conc. = 0.0338 Report level label = 0.01 Pct Recovery = 130% Analysis Date = 11/18/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6537100: 50 µl SpecificMix = EN170808006 Laboratory ID = 20161260151 Lab Value = 0.031 Expected Conc. = 0.032 Report level label = 0.01 Pct Recovery = 98% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = 3851600 Laboratory ID = 20151550293 Lab Value = 0.064 Expected Conc. = 0.032 Report level label = 0.01 Pct Recovery = 199% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl SpecificMix = 3851600 Laboratory ID = 20151270112 Lab Value = 0.036 Expected Conc. = 0.032 Report level label = 0.01 Pct Recovery = 112% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl SpecificMix = 3851600 Laboratory ID = 20160770090 Lab Value = 0.030 Expected Conc. = 0.0303 Report level label = 0.01 Pct Recovery = 97% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20160630046 Lab Value = 0.029 Expected Conc. = 0.0303 Report level label = 0.01 Pct Recovery = 96% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20153510109 Lab Value = 0.025 Expected Conc. = 0.0303 Report level label = 0.01 Pct Recovery = 84% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20153440001 Lab Value = 0.027 Expected Conc. = 0.0303 Report level label = 0.01 Pct Recovery = 88% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20171940002 Lab Value = 0.027 Expected Conc. = 0.0252 Report level label = 0.01 Pct Recovery = 108% Analysis Date = 11/10/17 SpikeMix = ChemService 5054800: 40 µl & NSI 041816: 40 µl SpecificMix = 041816 Laboratory ID = 20171160110 Lab Value = 0.026 Expected Conc. = 0.0252 Report level label = 0.01 Pct Recovery = 101% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = 060916 Laboratory ID = 20162520001 Lab Value = 0.033 Expected Conc. = 0.0252 Report level label = 0.01 Pct Recovery = 130% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl SpecificMix = 060916 Laboratory ID = 20163560019 Lab Value = 0.028 Expected Conc. = 0.0252 Report level label = 0.01 Pct Recovery = 113% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl SpecificMix = 060916 Laboratory ID = 20162380004 Lab Value = 0.024 Expected Conc. = 0.0252 Report level label = 0.01 Pct Recovery = 93% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = 060916 Laboratory ID = 20162020124 Lab Value = 0.019 Expected Conc. = 0.0252 Report level label = 0.01 Pct Recovery = 76% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl SpecificMix = 041816 Laboratory ID = 20161600087 Lab Value = 0.025 Expected Conc. = 0.0252 Report level label = 0.01 Pct Recovery = 97% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 041816 Laboratory ID = 20161340228 Lab Value = 0.025 Expected Conc. = 0.0252 Report level label = 0.01 Pct Recovery = 98% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl SpecificMix = 041816 Laboratory ID = 20161190075 Lab Value = 0.025 Expected Conc. = 0.0252 Report level label = 0.01 Pct Recovery = 100% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 041816 Laboratory ID = 20173120093 Lab Value = 0.023 Expected Conc. = 0.021 Report level label = 0.01 Pct Recovery = 108% Analysis Date = 03/10/18 SpikeMix = ChemService 6472100: 30 µl & ChemService 6537100: 30 µl SpecificMix = 6472100 Laboratory ID = 20150150115 Lab Value = 0.032 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 157% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl SpecificMix = 032714 Laboratory ID = 20142820151 Lab Value = 0.022 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 110% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl SpecificMix = 032714 Laboratory ID = 20141490205 Lab Value = 0.019 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 94% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = 032714 Laboratory ID = 20141080004 Lab Value = 0.021 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 106% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl SpecificMix = 032714 Laboratory ID = 20142470041 Lab Value = 0.022 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 108% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141910243 Lab Value = 0.017 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 83% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141640076 Lab Value = 0.017 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 84% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141360094 Lab Value = 0.016 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 81% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = E1140407002 Laboratory ID = 20160430111 Lab Value = 0.015 Expected Conc. = 0.016 Report level label = 0.01 Pct Recovery = 94% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 3851600 Laboratory ID = 20160210080 Lab Value = 0.014 Expected Conc. = 0.016 Report level label = 0.01 Pct Recovery = 89% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 3851600 Laboratory ID = 20152950078 Lab Value = 0.013 Expected Conc. = 0.016 Report level label = 0.01 Pct Recovery = 81% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 3851600 Laboratory ID = 20153030068 Lab Value = 0.016 Expected Conc. = 0.016 Report level label = 0.01 Pct Recovery = 103% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = 3851600 Laboratory ID = 20151760208 Lab Value = 0.028 Expected Conc. = 0.016 Report level label = 0.01 Pct Recovery = 178% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl SpecificMix = 3851600 Laboratory ID = 20151380009 Lab Value = 0.021 Expected Conc. = 0.016 Report level label = 0.01 Pct Recovery = 131% Analysis Date = 05/30/15 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 3851600 Laboratory ID = 20152040177 Lab Value = 0.024 Expected Conc. = 0.0152 Report level label = 0.01 Pct Recovery = 161% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl SpecificMix = 0406-15-01 Analysis Date = 03/10/18 Pct Recovery = 111% Analysis Date = 02/28/18 Pct Recovery = 110% Analysis Date = 02/28/18 Pct Recovery = 110% Analysis Date = 02/19/18 Pct Recovery = 110% Analysis Date = 02/19/18 Pct Recovery = 110% Analysis Date = 02/09/18 Pct Recovery = 110% Analysis Date = 02/09/18 Pct Recovery = 110% Analysis Date = 01/31/18 Pct Recovery = 110% Analysis Date = 01/31/18 Pct Recovery = 110% Analysis Date = 01/22/18 Pct Recovery = 109% Analysis Date = 01/22/18 Pct Recovery = 109% Analysis Date = 01/12/18 Pct Recovery = 109% Analysis Date = 01/12/18 Pct Recovery = 109% Analysis Date = 01/03/18 Pct Recovery = 109% Analysis Date = 01/03/18 Pct Recovery = 109% Analysis Date = 12/24/17 Pct Recovery = 108% Analysis Date = 12/24/17 Pct Recovery = 108% Analysis Date = 12/15/17 Pct Recovery = 108% Analysis Date = 12/15/17 Pct Recovery = 108% Analysis Date = 12/06/17 Pct Recovery = 108% Analysis Date = 12/06/17 Pct Recovery = 108% Analysis Date = 11/26/17 Pct Recovery = 107% Analysis Date = 11/26/17 Pct Recovery = 107% Analysis Date = 11/17/17 Pct Recovery = 107% Analysis Date = 11/17/17 Pct Recovery = 107% Analysis Date = 11/07/17 Pct Recovery = 107% Analysis Date = 11/07/17 Pct Recovery = 107% Analysis Date = 10/29/17 Pct Recovery = 107% Analysis Date = 10/29/17 Pct Recovery = 107% Analysis Date = 10/20/17 Pct Recovery = 106% Analysis Date = 10/20/17 Pct Recovery = 106% Analysis Date = 10/10/17 Pct Recovery = 106% Analysis Date = 10/10/17 Pct Recovery = 106% Analysis Date = 10/01/17 Pct Recovery = 106% Analysis Date = 10/01/17 Pct Recovery = 106% Analysis Date = 09/21/17 Pct Recovery = 105% Analysis Date = 09/21/17 Pct Recovery = 105% Analysis Date = 09/12/17 Pct Recovery = 105% Analysis Date = 09/12/17 Pct Recovery = 105% Analysis Date = 09/03/17 Pct Recovery = 105% Analysis Date = 09/03/17 Pct Recovery = 105% Analysis Date = 08/24/17 Pct Recovery = 105% Analysis Date = 08/24/17 Pct Recovery = 105% Analysis Date = 08/15/17 Pct Recovery = 104% Analysis Date = 08/15/17 Pct Recovery = 104% Analysis Date = 08/05/17 Pct Recovery = 104% Analysis Date = 08/05/17 Pct Recovery = 104% Analysis Date = 07/27/17 Pct Recovery = 104% Analysis Date = 07/27/17 Pct Recovery = 104% Analysis Date = 07/18/17 Pct Recovery = 103% Analysis Date = 07/18/17 Pct Recovery = 103% Analysis Date = 07/08/17 Pct Recovery = 103% Analysis Date = 07/08/17 Pct Recovery = 103% Analysis Date = 06/29/17 Pct Recovery = 103% Analysis Date = 06/29/17 Pct Recovery = 103% Analysis Date = 06/19/17 Pct Recovery = 103% Analysis Date = 06/19/17 Pct Recovery = 103% Analysis Date = 06/10/17 Pct Recovery = 102% Analysis Date = 06/10/17 Pct Recovery = 102% Analysis Date = 06/01/17 Pct Recovery = 102% Analysis Date = 06/01/17 Pct Recovery = 102% Analysis Date = 05/22/17 Pct Recovery = 102% Analysis Date = 05/22/17 Pct Recovery = 102% Analysis Date = 05/13/17 Pct Recovery = 101% Analysis Date = 05/13/17 Pct Recovery = 101% Analysis Date = 05/03/17 Pct Recovery = 101% Analysis Date = 05/03/17 Pct Recovery = 101% Analysis Date = 04/24/17 Pct Recovery = 101% Analysis Date = 04/24/17 Pct Recovery = 101% Analysis Date = 04/15/17 Pct Recovery = 101% Analysis Date = 04/15/17 Pct Recovery = 101% Analysis Date = 04/05/17 Pct Recovery = 100% Analysis Date = 04/05/17 Pct Recovery = 100% Analysis Date = 03/27/17 Pct Recovery = 100% Analysis Date = 03/27/17 Pct Recovery = 100% Analysis Date = 03/17/17 Pct Recovery = 100% Analysis Date = 03/17/17 Pct Recovery = 100% Analysis Date = 03/08/17 Pct Recovery = 100% Analysis Date = 03/08/17 Pct Recovery = 100% Analysis Date = 02/27/17 Pct Recovery = 99% Analysis Date = 02/27/17 Pct Recovery = 99% Analysis Date = 02/17/17 Pct Recovery = 99% Analysis Date = 02/17/17 Pct Recovery = 99% Analysis Date = 02/08/17 Pct Recovery = 99% Analysis Date = 02/08/17 Pct Recovery = 99% Analysis Date = 01/29/17 Pct Recovery = 98% Analysis Date = 01/29/17 Pct Recovery = 98% Analysis Date = 01/20/17 Pct Recovery = 98% Analysis Date = 01/20/17 Pct Recovery = 98% Analysis Date = 01/11/17 Pct Recovery = 98% Analysis Date = 01/11/17 Pct Recovery = 98% Analysis Date = 01/01/17 Pct Recovery = 98% Analysis Date = 01/01/17 Pct Recovery = 98% Analysis Date = 12/23/16 Pct Recovery = 97% Analysis Date = 12/23/16 Pct Recovery = 97% Analysis Date = 12/13/16 Pct Recovery = 97% Analysis Date = 12/13/16 Pct Recovery = 97% Analysis Date = 12/04/16 Pct Recovery = 97% Analysis Date = 12/04/16 Pct Recovery = 97% Analysis Date = 11/25/16 Pct Recovery = 97% Analysis Date = 11/25/16 Pct Recovery = 97% Analysis Date = 11/15/16 Pct Recovery = 97% Analysis Date = 11/15/16 Pct Recovery = 97% Analysis Date = 11/06/16 Pct Recovery = 97% Analysis Date = 11/06/16 Pct Recovery = 97% Analysis Date = 10/27/16 Pct Recovery = 97% Analysis Date = 10/27/16 Pct Recovery = 97% Analysis Date = 10/18/16 Pct Recovery = 96% Analysis Date = 10/18/16 Pct Recovery = 96% Analysis Date = 10/09/16 Pct Recovery = 96% Analysis Date = 10/09/16 Pct Recovery = 96% Analysis Date = 09/29/16 Pct Recovery = 96% Analysis Date = 09/29/16 Pct Recovery = 96% Analysis Date = 09/20/16 Pct Recovery = 96% Analysis Date = 09/20/16 Pct Recovery = 96% Analysis Date = 09/10/16 Pct Recovery = 96% Analysis Date = 09/10/16 Pct Recovery = 96% Analysis Date = 09/01/16 Pct Recovery = 96% Analysis Date = 09/01/16 Pct Recovery = 96% Analysis Date = 08/23/16 Pct Recovery = 96% Analysis Date = 08/23/16 Pct Recovery = 96% Analysis Date = 08/13/16 Pct Recovery = 97% Analysis Date = 08/13/16 Pct Recovery = 97% Analysis Date = 08/04/16 Pct Recovery = 98% Analysis Date = 08/04/16 Pct Recovery = 98% Analysis Date = 07/25/16 Pct Recovery = 99% Analysis Date = 07/25/16 Pct Recovery = 99% Analysis Date = 07/16/16 Pct Recovery = 100% Analysis Date = 07/16/16 Pct Recovery = 100% Analysis Date = 07/07/16 Pct Recovery = 101% Analysis Date = 07/07/16 Pct Recovery = 101% Analysis Date = 06/27/16 Pct Recovery = 102% Analysis Date = 06/27/16 Pct Recovery = 102% Analysis Date = 06/18/16 Pct Recovery = 103% Analysis Date = 06/18/16 Pct Recovery = 103% Analysis Date = 06/08/16 Pct Recovery = 104% Analysis Date = 06/08/16 Pct Recovery = 104% Analysis Date = 05/30/16 Pct Recovery = 104% Analysis Date = 05/30/16 Pct Recovery = 104% Analysis Date = 05/21/16 Pct Recovery = 105% Analysis Date = 05/21/16 Pct Recovery = 105% Analysis Date = 05/11/16 Pct Recovery = 106% Analysis Date = 05/11/16 Pct Recovery = 106% Analysis Date = 05/02/16 Pct Recovery = 107% Analysis Date = 05/02/16 Pct Recovery = 107% Analysis Date = 04/22/16 Pct Recovery = 108% Analysis Date = 04/22/16 Pct Recovery = 108% Analysis Date = 04/13/16 Pct Recovery = 109% Analysis Date = 04/13/16 Pct Recovery = 109% Analysis Date = 04/04/16 Pct Recovery = 110% Analysis Date = 04/04/16 Pct Recovery = 110% Analysis Date = 03/25/16 Pct Recovery = 110% Analysis Date = 03/25/16 Pct Recovery = 110% Analysis Date = 03/16/16 Pct Recovery = 111% Analysis Date = 03/16/16 Pct Recovery = 111% Analysis Date = 03/06/16 Pct Recovery = 112% Analysis Date = 03/06/16 Pct Recovery = 112% Analysis Date = 02/26/16 Pct Recovery = 113% Analysis Date = 02/26/16 Pct Recovery = 113% Analysis Date = 02/17/16 Pct Recovery = 114% Analysis Date = 02/17/16 Pct Recovery = 114% Analysis Date = 02/07/16 Pct Recovery = 114% Analysis Date = 02/07/16 Pct Recovery = 114% Analysis Date = 01/29/16 Pct Recovery = 115% Analysis Date = 01/29/16 Pct Recovery = 115% Analysis Date = 01/19/16 Pct Recovery = 116% Analysis Date = 01/19/16 Pct Recovery = 116% Analysis Date = 01/10/16 Pct Recovery = 117% Analysis Date = 01/10/16 Pct Recovery = 117% Analysis Date = 01/01/16 Pct Recovery = 118% Analysis Date = 01/01/16 Pct Recovery = 118% Analysis Date = 12/22/15 Pct Recovery = 119% Analysis Date = 12/22/15 Pct Recovery = 119% Analysis Date = 12/13/15 Pct Recovery = 120% Analysis Date = 12/13/15 Pct Recovery = 120% Analysis Date = 12/03/15 Pct Recovery = 121% Analysis Date = 12/03/15 Pct Recovery = 121% Analysis Date = 11/24/15 Pct Recovery = 122% Analysis Date = 11/24/15 Pct Recovery = 122% Analysis Date = 11/15/15 Pct Recovery = 123% Analysis Date = 11/15/15 Pct Recovery = 123% Analysis Date = 11/05/15 Pct Recovery = 124% Analysis Date = 11/05/15 Pct Recovery = 124% Analysis Date = 10/27/15 Pct Recovery = 125% Analysis Date = 10/27/15 Pct Recovery = 125% Analysis Date = 10/17/15 Pct Recovery = 126% Analysis Date = 10/17/15 Pct Recovery = 126% Analysis Date = 10/08/15 Pct Recovery = 127% Analysis Date = 10/08/15 Pct Recovery = 127% Analysis Date = 09/29/15 Pct Recovery = 128% Analysis Date = 09/29/15 Pct Recovery = 128% Analysis Date = 09/19/15 Pct Recovery = 129% Analysis Date = 09/19/15 Pct Recovery = 129% Analysis Date = 09/10/15 Pct Recovery = 129% Analysis Date = 09/10/15 Pct Recovery = 129% Analysis Date = 08/31/15 Pct Recovery = 130% Analysis Date = 08/31/15 Pct Recovery = 130% Analysis Date = 08/22/15 Pct Recovery = 131% Analysis Date = 08/22/15 Pct Recovery = 131% Analysis Date = 08/13/15 Pct Recovery = 132% Analysis Date = 08/13/15 Pct Recovery = 132% Analysis Date = 08/03/15 Pct Recovery = 133% Analysis Date = 08/03/15 Pct Recovery = 133% Analysis Date = 07/25/15 Pct Recovery = 134% Analysis Date = 07/25/15 Pct Recovery = 134% Analysis Date = 07/15/15 Pct Recovery = 134% Analysis Date = 07/15/15 Pct Recovery = 134% Analysis Date = 07/06/15 Pct Recovery = 135% Analysis Date = 07/06/15 Pct Recovery = 135% Analysis Date = 06/27/15 Pct Recovery = 135% Analysis Date = 06/27/15 Pct Recovery = 135% Analysis Date = 06/17/15 Pct Recovery = 136% Analysis Date = 06/17/15 Pct Recovery = 136% Analysis Date = 06/08/15 Pct Recovery = 137% Analysis Date = 06/08/15 Pct Recovery = 137% Analysis Date = 05/29/15 Pct Recovery = 137% Analysis Date = 05/29/15 Pct Recovery = 137% Analysis Date = 05/20/15 Pct Recovery = 138% Analysis Date = 05/20/15 Pct Recovery = 138% Analysis Date = 05/11/15 Pct Recovery = 138% Analysis Date = 05/11/15 Pct Recovery = 138% Analysis Date = 05/01/15 Pct Recovery = 137% Analysis Date = 05/01/15 Pct Recovery = 137% Analysis Date = 04/22/15 Pct Recovery = 136% Analysis Date = 04/22/15 Pct Recovery = 136% Analysis Date = 04/12/15 Pct Recovery = 134% Analysis Date = 04/12/15 Pct Recovery = 134% Analysis Date = 04/03/15 Pct Recovery = 133% Analysis Date = 04/03/15 Pct Recovery = 133% Analysis Date = 03/25/15 Pct Recovery = 132% Analysis Date = 03/25/15 Pct Recovery = 132% Analysis Date = 03/15/15 Pct Recovery = 131% Analysis Date = 03/15/15 Pct Recovery = 131% Analysis Date = 03/06/15 Pct Recovery = 130% Analysis Date = 03/06/15 Pct Recovery = 130% Analysis Date = 02/24/15 Pct Recovery = 128% Analysis Date = 02/24/15 Pct Recovery = 128% Analysis Date = 02/15/15 Pct Recovery = 127% Analysis Date = 02/15/15 Pct Recovery = 127% Analysis Date = 02/06/15 Pct Recovery = 126% Analysis Date = 02/06/15 Pct Recovery = 126% Analysis Date = 01/27/15 Pct Recovery = 125% Analysis Date = 01/27/15 Pct Recovery = 125% Analysis Date = 01/18/15 Pct Recovery = 124% Analysis Date = 01/18/15 Pct Recovery = 124% Analysis Date = 01/08/15 Pct Recovery = 122% Analysis Date = 01/08/15 Pct Recovery = 122% Analysis Date = 12/30/14 Pct Recovery = 121% Analysis Date = 12/30/14 Pct Recovery = 121% Analysis Date = 12/21/14 Pct Recovery = 120% Analysis Date = 12/21/14 Pct Recovery = 120% Analysis Date = 12/11/14 Pct Recovery = 119% Analysis Date = 12/11/14 Pct Recovery = 119% Analysis Date = 12/02/14 Pct Recovery = 118% Analysis Date = 12/02/14 Pct Recovery = 118% Analysis Date = 11/22/14 Pct Recovery = 116% Analysis Date = 11/22/14 Pct Recovery = 116% Analysis Date = 11/13/14 Pct Recovery = 115% Analysis Date = 11/13/14 Pct Recovery = 115% Analysis Date = 11/04/14 Pct Recovery = 113% Analysis Date = 11/04/14 Pct Recovery = 113% Analysis Date = 10/25/14 Pct Recovery = 112% Analysis Date = 10/25/14 Pct Recovery = 112% Analysis Date = 10/16/14 Pct Recovery = 111% Analysis Date = 10/16/14 Pct Recovery = 111% Analysis Date = 10/06/14 Pct Recovery = 109% Analysis Date = 10/06/14 Pct Recovery = 109% Analysis Date = 09/27/14 Pct Recovery = 108% Analysis Date = 09/27/14 Pct Recovery = 108% Analysis Date = 09/18/14 Pct Recovery = 107% Analysis Date = 09/18/14 Pct Recovery = 107% Analysis Date = 09/08/14 Pct Recovery = 106% Analysis Date = 09/08/14 Pct Recovery = 106% Analysis Date = 08/30/14 Pct Recovery = 105% Analysis Date = 08/30/14 Pct Recovery = 105% Analysis Date = 08/20/14 Pct Recovery = 104% Analysis Date = 08/20/14 Pct Recovery = 104% Analysis Date = 08/11/14 Pct Recovery = 103% Analysis Date = 08/11/14 Pct Recovery = 103% Analysis Date = 08/02/14 Pct Recovery = 102% Analysis Date = 08/02/14 Pct Recovery = 102% Analysis Date = 07/23/14 Pct Recovery = 101% Analysis Date = 07/23/14 Pct Recovery = 101% Analysis Date = 07/14/14 Pct Recovery = 100% Analysis Date = 07/14/14 Pct Recovery = 100% Analysis Date = 07/04/14 Pct Recovery = 99% Analysis Date = 07/04/14 Pct Recovery = 99% Analysis Date = 06/25/14 Pct Recovery = 99% Analysis Date = 06/25/14 Pct Recovery = 99% Analysis Date = 06/16/14 Pct Recovery = 99% Analysis Date = 06/16/14 Pct Recovery = 99% Analysis Date = 06/06/14 Pct Recovery = 99% Analysis Date = 06/06/14 Pct Recovery = 99% Analysis Date = 05/28/14 Pct Recovery = 99% Analysis Date = 05/28/14 Pct Recovery = 99% Analysis Date = 05/18/14 Pct Recovery = 98% Analysis Date = 05/18/14 Pct Recovery = 98% Analysis Date = 05/09/14 Pct Recovery = 98% Analysis Date = 05/09/14 Pct Recovery = 98% Analysis Date = 04/30/14 Pct Recovery = 97% Analysis Date = 04/30/14 Pct Recovery = 97% Analysis Date = 04/20/14 Pct Recovery = 97% Analysis Date = 04/20/14 Pct Recovery = 97% Analysis Date = 04/11/14 Pct Recovery = 96% Analysis Date = 04/11/14 Pct Recovery = 96% Analysis Date = 04/01/14 Pct Recovery = 95% Analysis Date = 04/01/14 Pct Recovery = 95% Analysis Date = 03/23/14 Pct Recovery = 95% Analysis Date = 03/23/14 Pct Recovery = 95% Analysis Date = 03/14/14 Pct Recovery = 94% Analysis Date = 03/14/14 Pct Recovery = 94% Analysis Date = 03/04/14 Pct Recovery = 94% Analysis Date = 03/04/14 Pct Recovery = 94% Analysis Date = 02/23/14 Pct Recovery = 93% Analysis Date = 02/23/14 Pct Recovery = 93% Analysis Date = 02/13/14 Pct Recovery = 92% Analysis Date = 02/13/14 Pct Recovery = 92% Analysis Date = 02/04/14 Pct Recovery = 92% Analysis Date = 02/04/14 Pct Recovery = 92% Analysis Date = 01/26/14 Pct Recovery = 91% Analysis Date = 01/26/14 Pct Recovery = 91% Analysis Date = 01/16/14 Pct Recovery = 91% Analysis Date = 01/16/14 Pct Recovery = 91% Analysis Date = 01/07/14 Pct Recovery = 90% Analysis Date = 01/07/14 Pct Recovery = 90% Analysis Date = 12/28/13 Pct Recovery = 89% Analysis Date = 12/28/13 Pct Recovery = 89% Analysis Date = 12/19/13 Pct Recovery = 89% Analysis Date = 12/19/13 Pct Recovery = 89% Analysis Date = 12/10/13 Pct Recovery = 88% Analysis Date = 12/10/13 Pct Recovery = 88% Analysis Date = 11/30/13 Pct Recovery = 88% Analysis Date = 11/30/13 Pct Recovery = 88% Analysis Date = 11/21/13 Pct Recovery = 87% Analysis Date = 11/21/13 Pct Recovery = 87% Analysis Date = 11/11/13 Pct Recovery = 87% Analysis Date = 11/11/13 Pct Recovery = 87% Analysis Date = 11/02/13 Pct Recovery = 86% Analysis Date = 11/02/13 Pct Recovery = 86% Analysis Date = 10/24/13 Pct Recovery = 85% Analysis Date = 10/24/13 Pct Recovery = 85% Analysis Date = 10/14/13 Pct Recovery = 85% Analysis Date = 10/14/13 Pct Recovery = 85% Analysis Date = 10/05/13 Pct Recovery = 84% Analysis Date = 10/05/13 Pct Recovery = 84% Analysis Date = 09/25/13 Pct Recovery = 84% Analysis Date = 09/25/13 Pct Recovery = 84% Analysis Date = 09/16/13 Pct Recovery = 83% Analysis Date = 09/16/13 Pct Recovery = 83% Analysis Date = 09/07/13 Pct Recovery = 82% Analysis Date = 09/07/13 Pct Recovery = 82% Analysis Date = 08/28/13 Pct Recovery = 82% Analysis Date = 08/28/13 Pct Recovery = 82% Analysis Date = 08/19/13 Pct Recovery = 81% Analysis Date = 08/19/13 Pct Recovery = 81% Analysis Date = 08/09/13 Pct Recovery = 81% Analysis Date = 08/09/13 Pct Recovery = 81% Analysis Date = 07/31/13 Pct Recovery = 80% Analysis Date = 07/31/13 Pct Recovery = 80% Analysis Date = 07/22/13 Pct Recovery = 79% Analysis Date = 07/22/13 Pct Recovery = 79% Analysis Date = 07/12/13 Pct Recovery = 79% Analysis Date = 07/12/13 Pct Recovery = 79% Analysis Date = 07/03/13 Pct Recovery = 78% Analysis Date = 07/03/13 Pct Recovery = 78% Analysis Date = 06/23/13 Pct Recovery = 78% Analysis Date = 06/23/13 Pct Recovery = 78% Analysis Date = 06/14/13 Pct Recovery = 77% Analysis Date = 06/14/13 Pct Recovery = 77% Analysis Date = 06/05/13 Pct Recovery = 77% Analysis Date = 06/05/13 Pct Recovery = 77% Analysis Date = 05/26/13 Pct Recovery = 76% Analysis Date = 05/26/13 Pct Recovery = 76% Analysis Date = 05/17/13 Pct Recovery = 75% Analysis Date = 05/17/13 Pct Recovery = 75% Analysis Date = 05/07/13 Pct Recovery = 75% Analysis Date = 05/07/13 Pct Recovery = 75% Analysis Date = 04/28/13 Pct Recovery = 74% Analysis Date = 04/28/13 Pct Recovery = 74% Analysis Date = 04/19/13 Pct Recovery = 74% Analysis Date = 04/19/13 Pct Recovery = 74% Analysis Date = 04/09/13 Pct Recovery = 73% Analysis Date = 04/09/13 Pct Recovery = 73% Analysis Date = 03/31/13 Pct Recovery = 72% Analysis Date = 03/31/13 Pct Recovery = 72% Analysis Date = 03/21/13 Pct Recovery = 72% Analysis Date = 03/21/13 Pct Recovery = 72% Analysis Date = 03/12/13 Pct Recovery = 71% Analysis Date = 03/12/13 Pct Recovery = 71% Analysis Date = 03/03/13 Pct Recovery = 71% Analysis Date = 03/03/13 Pct Recovery = 71% Analysis Date = 02/21/13 Pct Recovery = 70% Analysis Date = 02/21/13 Pct Recovery = 70% Analysis Date = 02/12/13 Pct Recovery = 70% Analysis Date = 02/12/13 Pct Recovery = 70% Analysis Date = 02/02/13 Pct Recovery = 69% Analysis Date = 02/02/13 Pct Recovery = 69% Analysis Date = 01/24/13 Pct Recovery = 68% Analysis Date = 01/24/13 Pct Recovery = 68% Analysis Date = 01/15/13 Pct Recovery = 68% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
DISULFOTON SULFONE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 58 106% 38% 97% 17%
Total 58 106% 38% 97% 17%

Sample Statistics
DISULFOTON SULFONE

Characteristic N % % Basis
Plotted 58 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 58 .  
False Negatives 0 0% 0 out of 58
Not Spiked 54 .  
False Positives 4 7% 4 out of 54

OBSP Determination:
ENDOSULFAN SULFATE
METHOD: 2033 , TESTIDCODE: 61590GCM39

Laboratory ID = 20130940097 Lab Value = 0.187 Expected Conc. = 0.2535 Report level label = 0.016 Pct Recovery = 74% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = 0507-12-04.2 Laboratory ID = 20123560092 Lab Value = 0.219 Expected Conc. = 0.2535 Report level label = 0.016 Pct Recovery = 86% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = 0507-12-04.2 Laboratory ID = 20130810108 Lab Value = 0.208 Expected Conc. = 0.25 Report level label = 0.016 Pct Recovery = 83% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl SpecificMix = LB92783 Laboratory ID = 20130100066 Lab Value = 0.211 Expected Conc. = 0.25 Report level label = 0.016 Pct Recovery = 84% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl SpecificMix = LB92783 Laboratory ID = 20132490342 Lab Value = 0.150 Expected Conc. = 0.2 Report level label = 0.016 Pct Recovery = 75% Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20172510330 Lab Value = 0.073 Expected Conc. = 0.107 Report level label = 0.016 Pct Recovery = 68% Analysis Date = 12/29/17 SpikeMix = ChemService 6537100: 100 µl & Abs 071817Pest: 100 µl SpecificMix = 071817Pest Laboratory ID = 20130510051 Lab Value = 0.091 Expected Conc. = 0.1014 Report level label = 0.016 Pct Recovery = 89% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl SpecificMix = 0507-12-04.2 Laboratory ID = 20163370001 Lab Value = 0.101 Expected Conc. = 0.1 Report level label = 0.016 Pct Recovery = 101% Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl SpecificMix = B20160331 Laboratory ID = 20163150006 Lab Value = 0.081 Expected Conc. = 0.1 Report level label = 0.016 Pct Recovery = 80% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl SpecificMix = B20160331 Laboratory ID = 20161880109 Lab Value = 0.096 Expected Conc. = 0.1 Report level label = 0.016 Pct Recovery = 96% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl SpecificMix = 03FF076 Laboratory ID = 20140370077 Lab Value = 0.077 Expected Conc. = 0.1 Report level label = 0.016 Pct Recovery = 77% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20132560001 Lab Value = 0.079 Expected Conc. = 0.1 Report level label = 0.016 Pct Recovery = 79% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20132140002 Lab Value = 0.080 Expected Conc. = 0.1 Report level label = 0.016 Pct Recovery = 80% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl SpecificMix = LB99392 Laboratory ID = 20131370001 Lab Value = 0.125 Expected Conc. = 0.1 Report level label = 0.016 Pct Recovery = 125% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl SpecificMix = LB99392 Laboratory ID = 20130390105 Lab Value = 0.075 Expected Conc. = 0.1 Report level label = 0.016 Pct Recovery = 75% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl SpecificMix = LB92783 Laboratory ID = 20152750006 Lab Value = 0.060 Expected Conc. = 0.0968 Report level label = 0.016 Pct Recovery = 62% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl SpecificMix = 040615 Laboratory ID = 20152610011 Lab Value = 0.097 Expected Conc. = 0.0968 Report level label = 0.016 Pct Recovery = 100% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl SpecificMix = 040615 Laboratory ID = 20171720140 Lab Value = 0.080 Expected Conc. = 0.08 Report level label = 0.016 Pct Recovery = 100% Analysis Date = 08/31/17 SpikeMix = Supelco LC20138V: 80 µl & Phenova B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20171660002 Lab Value = 0.080 Expected Conc. = 0.08 Report level label = 0.016 Pct Recovery = 100% Analysis Date = 08/23/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20170960001 Lab Value = 0.057 Expected Conc. = 0.08 Report level label = 0.016 Pct Recovery = 71% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl SpecificMix = 03FF076 Laboratory ID = 20170190026 Lab Value = 0.071 Expected Conc. = 0.08 Report level label = 0.016 Pct Recovery = 88% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20161470001 Lab Value = 0.066 Expected Conc. = 0.08 Report level label = 0.016 Pct Recovery = 83% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20150430092 Lab Value = 0.052 Expected Conc. = 0.066 Report level label = 0.016 Pct Recovery = 79% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl SpecificMix = E1140407002 Laboratory ID = 20143110108 Lab Value = 0.042 Expected Conc. = 0.066 Report level label = 0.016 Pct Recovery = 64% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl SpecificMix = E1140407002 Laboratory ID = 20142720002 Lab Value = 0.050 Expected Conc. = 0.066 Report level label = 0.016 Pct Recovery = 75% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl SpecificMix = E1140407002 Laboratory ID = 20141770149 Lab Value = 0.047 Expected Conc. = 0.066 Report level label = 0.016 Pct Recovery = 72% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl SpecificMix = E1140407002 Laboratory ID = 20143240095 Lab Value = 0.045 Expected Conc. = 0.0648 Report level label = 0.016 Pct Recovery = 70% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl SpecificMix = 032714 Laboratory ID = 20142270001 Lab Value = 0.046 Expected Conc. = 0.0648 Report level label = 0.016 Pct Recovery = 72% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl SpecificMix = 032714 Laboratory ID = 20141220025 Lab Value = 0.050 Expected Conc. = 0.0648 Report level label = 0.016 Pct Recovery = 78% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl SpecificMix = 032714 Laboratory ID = 20172560101 Lab Value = 0.041 Expected Conc. = 0.055 Report level label = 0.016 Pct Recovery = 75% Analysis Date = 12/22/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6567600: 50 µl SpecificMix = 6567600 Laboratory ID = 20151900132 Lab Value = 0.031 Expected Conc. = 0.0484 Report level label = 0.016 Pct Recovery = 65% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl SpecificMix = 040615 Laboratory ID = 20151550293 Lab Value = 0.040 Expected Conc. = 0.0484 Report level label = 0.016 Pct Recovery = 83% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl SpecificMix = 040615 Laboratory ID = 20161260151 Lab Value = 0.033 Expected Conc. = 0.048 Report level label = 0.016 Pct Recovery = 68% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = EN150513008 Laboratory ID = 20160770090 Lab Value = 0.033 Expected Conc. = 0.048 Report level label = 0.016 Pct Recovery = 69% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = EN150513008 Laboratory ID = 20153510109 Lab Value = 0.037 Expected Conc. = 0.048 Report level label = 0.016 Pct Recovery = 77% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = EN150513008 Laboratory ID = 20152330039 Lab Value = 0.039 Expected Conc. = 0.048 Report level label = 0.016 Pct Recovery = 81% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl SpecificMix = EN150513008 Laboratory ID = 20172020035 Lab Value = 0.039 Expected Conc. = 0.04 Report level label = 0.016 Pct Recovery = 98% Analysis Date = 11/07/17 SpikeMix = Abs 071717Pest: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20171510080 Lab Value = 0.037 Expected Conc. = 0.04 Report level label = 0.016 Pct Recovery = 92% Analysis Date = 06/09/17 SpikeMix = Supelco LC20138V: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20171160110 Lab Value = 0.040 Expected Conc. = 0.04 Report level label = 0.016 Pct Recovery = 100% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = B20160331 Laboratory ID = 20170460061 Lab Value = 0.031 Expected Conc. = 0.04 Report level label = 0.016 Pct Recovery = 77% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl SpecificMix = 03FF076 Laboratory ID = 20162660005 Lab Value = 0.036 Expected Conc. = 0.04 Report level label = 0.016 Pct Recovery = 90% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl SpecificMix = 03FF076 Laboratory ID = 20162380004 Lab Value = 0.034 Expected Conc. = 0.04 Report level label = 0.016 Pct Recovery = 86% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = B20160331 Laboratory ID = 20162150213 Lab Value = 0.047 Expected Conc. = 0.04 Report level label = 0.016 Pct Recovery = 117% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl SpecificMix = B20160331 Laboratory ID = 20161600087 Lab Value = 0.029 Expected Conc. = 0.04 Report level label = 0.016 Pct Recovery = 73% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20161340228 Lab Value = 0.029 Expected Conc. = 0.04 Report level label = 0.016 Pct Recovery = 73% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl SpecificMix = 03FF076 Laboratory ID = 20161190075 Lab Value = 0.029 Expected Conc. = 0.04 Report level label = 0.016 Pct Recovery = 72% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20140510043 Lab Value = 0.034 Expected Conc. = 0.04 Report level label = 0.016 Pct Recovery = 85% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl SpecificMix = LB99392 Laboratory ID = 20133580036 Lab Value = 0.029 Expected Conc. = 0.04 Report level label = 0.016 Pct Recovery = 73% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20133470008 Lab Value = 0.036 Expected Conc. = 0.04 Report level label = 0.016 Pct Recovery = 90% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl SpecificMix = LB99392 Laboratory ID = 20133190012 Lab Value = 0.039 Expected Conc. = 0.04 Report level label = 0.016 Pct Recovery = 97% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = LB99392 Laboratory ID = 20133050050 Lab Value = 0.034 Expected Conc. = 0.04 Report level label = 0.016 Pct Recovery = 86% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl SpecificMix = LB99392 Laboratory ID = 20131790009 Lab Value = 0.025 Expected Conc. = 0.04 Report level label = 0.016 Pct Recovery = 62% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20131510026 Lab Value = 0.039 Expected Conc. = 0.04 Report level label = 0.016 Pct Recovery = 98% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20142470041 Lab Value = 0.023 Expected Conc. = 0.033 Report level label = 0.016 Pct Recovery = 68% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141910243 Lab Value = 0.022 Expected Conc. = 0.033 Report level label = 0.016 Pct Recovery = 67% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141640076 Lab Value = 0.017 Expected Conc. = 0.033 Report level label = 0.016 Pct Recovery = 51% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141360094 Lab Value = 0.023 Expected Conc. = 0.033 Report level label = 0.016 Pct Recovery = 69% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = E1140407002 Laboratory ID = 20150150115 Lab Value = 0.023 Expected Conc. = 0.0324 Report level label = 0.016 Pct Recovery = 71% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl SpecificMix = 032714 Laboratory ID = 20142820151 Lab Value = 0.024 Expected Conc. = 0.0324 Report level label = 0.016 Pct Recovery = 73% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl SpecificMix = 032714 Laboratory ID = 20141490205 Lab Value = 0.021 Expected Conc. = 0.0324 Report level label = 0.016 Pct Recovery = 64% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = 032714 Laboratory ID = 20141080004 Lab Value = 0.020 Expected Conc. = 0.0324 Report level label = 0.016 Pct Recovery = 60% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl SpecificMix = 032714 Laboratory ID = 20172780018 Lab Value = 0.036 Expected Conc. = 0.0321 Report level label = 0.016 Pct Recovery = 112% Analysis Date = 02/08/18 SpikeMix = ChemService 6537100: 30 µl & Abs 071817Pest: 30 µl SpecificMix = 071817Pest Laboratory ID = 20161050143 Lab Value = 0.017 Expected Conc. = 0.0242 Report level label = 0.016 Pct Recovery = 71% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Laboratory ID = 20160430111 Lab Value = 0.020 Expected Conc. = 0.0242 Report level label = 0.016 Pct Recovery = 82% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Laboratory ID = 20160070059 Lab Value = 0.022 Expected Conc. = 0.0242 Report level label = 0.016 Pct Recovery = 89% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = 040615 Laboratory ID = 20151380009 Lab Value = 0.015 Expected Conc. = 0.0242 Report level label = 0.016 Pct Recovery = 60% Analysis Date = 05/30/15 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Laboratory ID = 20151210037 Lab Value = 0.019 Expected Conc. = 0.0242 Report level label = 0.016 Pct Recovery = 76% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Laboratory ID = 20160560044 Lab Value = 0.019 Expected Conc. = 0.024 Report level label = 0.016 Pct Recovery = 80% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl SpecificMix = EN150513008 Laboratory ID = 20153160001 Lab Value = 0.016 Expected Conc. = 0.024 Report level label = 0.016 Pct Recovery = 66% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = EN150513008 Laboratory ID = 20153030068 Lab Value = 0.018 Expected Conc. = 0.024 Report level label = 0.016 Pct Recovery = 75% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150513008 Laboratory ID = 20152190003 Lab Value = 0.017 Expected Conc. = 0.024 Report level label = 0.016 Pct Recovery = 69% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150513008 Laboratory ID = 20151480170 Lab Value = 0.020 Expected Conc. = 0.024 Report level label = 0.016 Pct Recovery = 85% Analysis Date = 06/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150513008 Analysis Date = 02/08/18 Pct Recovery = 94% Analysis Date = 01/29/18 Pct Recovery = 94% Analysis Date = 01/29/18 Pct Recovery = 94% Analysis Date = 01/20/18 Pct Recovery = 94% Analysis Date = 01/20/18 Pct Recovery = 94% Analysis Date = 01/11/18 Pct Recovery = 94% Analysis Date = 01/11/18 Pct Recovery = 94% Analysis Date = 01/02/18 Pct Recovery = 94% Analysis Date = 01/02/18 Pct Recovery = 94% Analysis Date = 12/23/17 Pct Recovery = 93% Analysis Date = 12/23/17 Pct Recovery = 93% Analysis Date = 12/14/17 Pct Recovery = 93% Analysis Date = 12/14/17 Pct Recovery = 93% Analysis Date = 12/05/17 Pct Recovery = 93% Analysis Date = 12/05/17 Pct Recovery = 93% Analysis Date = 11/26/17 Pct Recovery = 93% Analysis Date = 11/26/17 Pct Recovery = 93% Analysis Date = 11/16/17 Pct Recovery = 93% Analysis Date = 11/16/17 Pct Recovery = 93% Analysis Date = 11/07/17 Pct Recovery = 92% Analysis Date = 11/07/17 Pct Recovery = 92% Analysis Date = 10/29/17 Pct Recovery = 92% Analysis Date = 10/29/17 Pct Recovery = 92% Analysis Date = 10/20/17 Pct Recovery = 92% Analysis Date = 10/20/17 Pct Recovery = 92% Analysis Date = 10/10/17 Pct Recovery = 92% Analysis Date = 10/10/17 Pct Recovery = 92% Analysis Date = 10/01/17 Pct Recovery = 92% Analysis Date = 10/01/17 Pct Recovery = 92% Analysis Date = 09/22/17 Pct Recovery = 91% Analysis Date = 09/22/17 Pct Recovery = 91% Analysis Date = 09/13/17 Pct Recovery = 91% Analysis Date = 09/13/17 Pct Recovery = 91% Analysis Date = 09/03/17 Pct Recovery = 91% Analysis Date = 09/03/17 Pct Recovery = 91% Analysis Date = 08/25/17 Pct Recovery = 91% Analysis Date = 08/25/17 Pct Recovery = 91% Analysis Date = 08/16/17 Pct Recovery = 90% Analysis Date = 08/16/17 Pct Recovery = 90% Analysis Date = 08/07/17 Pct Recovery = 90% Analysis Date = 08/07/17 Pct Recovery = 90% Analysis Date = 07/28/17 Pct Recovery = 90% Analysis Date = 07/28/17 Pct Recovery = 90% Analysis Date = 07/19/17 Pct Recovery = 90% Analysis Date = 07/19/17 Pct Recovery = 90% Analysis Date = 07/10/17 Pct Recovery = 90% Analysis Date = 07/10/17 Pct Recovery = 90% Analysis Date = 07/01/17 Pct Recovery = 89% Analysis Date = 07/01/17 Pct Recovery = 89% Analysis Date = 06/21/17 Pct Recovery = 89% Analysis Date = 06/21/17 Pct Recovery = 89% Analysis Date = 06/12/17 Pct Recovery = 89% Analysis Date = 06/12/17 Pct Recovery = 89% Analysis Date = 06/03/17 Pct Recovery = 89% Analysis Date = 06/03/17 Pct Recovery = 89% Analysis Date = 05/25/17 Pct Recovery = 89% Analysis Date = 05/25/17 Pct Recovery = 89% Analysis Date = 05/15/17 Pct Recovery = 88% Analysis Date = 05/15/17 Pct Recovery = 88% Analysis Date = 05/06/17 Pct Recovery = 88% Analysis Date = 05/06/17 Pct Recovery = 88% Analysis Date = 04/27/17 Pct Recovery = 88% Analysis Date = 04/27/17 Pct Recovery = 88% Analysis Date = 04/18/17 Pct Recovery = 88% Analysis Date = 04/18/17 Pct Recovery = 88% Analysis Date = 04/08/17 Pct Recovery = 88% Analysis Date = 04/08/17 Pct Recovery = 88% Analysis Date = 03/30/17 Pct Recovery = 87% Analysis Date = 03/30/17 Pct Recovery = 87% Analysis Date = 03/21/17 Pct Recovery = 87% Analysis Date = 03/21/17 Pct Recovery = 87% Analysis Date = 03/12/17 Pct Recovery = 87% Analysis Date = 03/12/17 Pct Recovery = 87% Analysis Date = 03/02/17 Pct Recovery = 87% Analysis Date = 03/02/17 Pct Recovery = 87% Analysis Date = 02/21/17 Pct Recovery = 86% Analysis Date = 02/21/17 Pct Recovery = 86% Analysis Date = 02/12/17 Pct Recovery = 86% Analysis Date = 02/12/17 Pct Recovery = 86% Analysis Date = 02/03/17 Pct Recovery = 86% Analysis Date = 02/03/17 Pct Recovery = 86% Analysis Date = 01/24/17 Pct Recovery = 86% Analysis Date = 01/24/17 Pct Recovery = 86% Analysis Date = 01/15/17 Pct Recovery = 86% Analysis Date = 01/15/17 Pct Recovery = 86% Analysis Date = 01/06/17 Pct Recovery = 85% Analysis Date = 01/06/17 Pct Recovery = 85% Analysis Date = 12/28/16 Pct Recovery = 85% Analysis Date = 12/28/16 Pct Recovery = 85% Analysis Date = 12/18/16 Pct Recovery = 85% Analysis Date = 12/18/16 Pct Recovery = 85% Analysis Date = 12/09/16 Pct Recovery = 85% Analysis Date = 12/09/16 Pct Recovery = 85% Analysis Date = 11/30/16 Pct Recovery = 85% Analysis Date = 11/30/16 Pct Recovery = 85% Analysis Date = 11/21/16 Pct Recovery = 84% Analysis Date = 11/21/16 Pct Recovery = 84% Analysis Date = 11/11/16 Pct Recovery = 84% Analysis Date = 11/11/16 Pct Recovery = 84% Analysis Date = 11/02/16 Pct Recovery = 84% Analysis Date = 11/02/16 Pct Recovery = 84% Analysis Date = 10/24/16 Pct Recovery = 84% Analysis Date = 10/24/16 Pct Recovery = 84% Analysis Date = 10/15/16 Pct Recovery = 84% Analysis Date = 10/15/16 Pct Recovery = 84% Analysis Date = 10/05/16 Pct Recovery = 83% Analysis Date = 10/05/16 Pct Recovery = 83% Analysis Date = 09/26/16 Pct Recovery = 83% Analysis Date = 09/26/16 Pct Recovery = 83% Analysis Date = 09/17/16 Pct Recovery = 83% Analysis Date = 09/17/16 Pct Recovery = 83% Analysis Date = 09/08/16 Pct Recovery = 83% Analysis Date = 09/08/16 Pct Recovery = 83% Analysis Date = 08/29/16 Pct Recovery = 83% Analysis Date = 08/29/16 Pct Recovery = 83% Analysis Date = 08/20/16 Pct Recovery = 82% Analysis Date = 08/20/16 Pct Recovery = 82% Analysis Date = 08/11/16 Pct Recovery = 82% Analysis Date = 08/11/16 Pct Recovery = 82% Analysis Date = 08/02/16 Pct Recovery = 82% Analysis Date = 08/02/16 Pct Recovery = 82% Analysis Date = 07/23/16 Pct Recovery = 82% Analysis Date = 07/23/16 Pct Recovery = 82% Analysis Date = 07/14/16 Pct Recovery = 82% Analysis Date = 07/14/16 Pct Recovery = 82% Analysis Date = 07/05/16 Pct Recovery = 81% Analysis Date = 07/05/16 Pct Recovery = 81% Analysis Date = 06/26/16 Pct Recovery = 81% Analysis Date = 06/26/16 Pct Recovery = 81% Analysis Date = 06/16/16 Pct Recovery = 81% Analysis Date = 06/16/16 Pct Recovery = 81% Analysis Date = 06/07/16 Pct Recovery = 81% Analysis Date = 06/07/16 Pct Recovery = 81% Analysis Date = 05/29/16 Pct Recovery = 81% Analysis Date = 05/29/16 Pct Recovery = 81% Analysis Date = 05/20/16 Pct Recovery = 80% Analysis Date = 05/20/16 Pct Recovery = 80% Analysis Date = 05/10/16 Pct Recovery = 80% Analysis Date = 05/10/16 Pct Recovery = 80% Analysis Date = 05/01/16 Pct Recovery = 80% Analysis Date = 05/01/16 Pct Recovery = 80% Analysis Date = 04/22/16 Pct Recovery = 80% Analysis Date = 04/22/16 Pct Recovery = 80% Analysis Date = 04/13/16 Pct Recovery = 80% Analysis Date = 04/13/16 Pct Recovery = 80% Analysis Date = 04/03/16 Pct Recovery = 79% Analysis Date = 04/03/16 Pct Recovery = 79% Analysis Date = 03/25/16 Pct Recovery = 79% Analysis Date = 03/25/16 Pct Recovery = 79% Analysis Date = 03/16/16 Pct Recovery = 79% Analysis Date = 03/16/16 Pct Recovery = 79% Analysis Date = 03/07/16 Pct Recovery = 79% Analysis Date = 03/07/16 Pct Recovery = 79% Analysis Date = 02/26/16 Pct Recovery = 79% Analysis Date = 02/26/16 Pct Recovery = 79% Analysis Date = 02/17/16 Pct Recovery = 78% Analysis Date = 02/17/16 Pct Recovery = 78% Analysis Date = 02/08/16 Pct Recovery = 78% Analysis Date = 02/08/16 Pct Recovery = 78% Analysis Date = 01/30/16 Pct Recovery = 78% Analysis Date = 01/30/16 Pct Recovery = 78% Analysis Date = 01/20/16 Pct Recovery = 78% Analysis Date = 01/20/16 Pct Recovery = 78% Analysis Date = 01/11/16 Pct Recovery = 78% Analysis Date = 01/11/16 Pct Recovery = 78% Analysis Date = 01/02/16 Pct Recovery = 77% Analysis Date = 01/02/16 Pct Recovery = 77% Analysis Date = 12/24/15 Pct Recovery = 77% Analysis Date = 12/24/15 Pct Recovery = 77% Analysis Date = 12/14/15 Pct Recovery = 77% Analysis Date = 12/14/15 Pct Recovery = 77% Analysis Date = 12/05/15 Pct Recovery = 77% Analysis Date = 12/05/15 Pct Recovery = 77% Analysis Date = 11/26/15 Pct Recovery = 77% Analysis Date = 11/26/15 Pct Recovery = 77% Analysis Date = 11/17/15 Pct Recovery = 76% Analysis Date = 11/17/15 Pct Recovery = 76% Analysis Date = 11/07/15 Pct Recovery = 76% Analysis Date = 11/07/15 Pct Recovery = 76% Analysis Date = 10/29/15 Pct Recovery = 76% Analysis Date = 10/29/15 Pct Recovery = 76% Analysis Date = 10/20/15 Pct Recovery = 76% Analysis Date = 10/20/15 Pct Recovery = 76% Analysis Date = 10/11/15 Pct Recovery = 76% Analysis Date = 10/11/15 Pct Recovery = 76% Analysis Date = 10/01/15 Pct Recovery = 75% Analysis Date = 10/01/15 Pct Recovery = 75% Analysis Date = 09/22/15 Pct Recovery = 75% Analysis Date = 09/22/15 Pct Recovery = 75% Analysis Date = 09/13/15 Pct Recovery = 75% Analysis Date = 09/13/15 Pct Recovery = 75% Analysis Date = 09/04/15 Pct Recovery = 75% Analysis Date = 09/04/15 Pct Recovery = 75% Analysis Date = 08/25/15 Pct Recovery = 75% Analysis Date = 08/25/15 Pct Recovery = 75% Analysis Date = 08/16/15 Pct Recovery = 75% Analysis Date = 08/16/15 Pct Recovery = 75% Analysis Date = 08/07/15 Pct Recovery = 75% Analysis Date = 08/07/15 Pct Recovery = 75% Analysis Date = 07/29/15 Pct Recovery = 74% Analysis Date = 07/29/15 Pct Recovery = 74% Analysis Date = 07/19/15 Pct Recovery = 74% Analysis Date = 07/19/15 Pct Recovery = 74% Analysis Date = 07/10/15 Pct Recovery = 74% Analysis Date = 07/10/15 Pct Recovery = 74% Analysis Date = 07/01/15 Pct Recovery = 74% Analysis Date = 07/01/15 Pct Recovery = 74% Analysis Date = 06/22/15 Pct Recovery = 74% Analysis Date = 06/22/15 Pct Recovery = 74% Analysis Date = 06/12/15 Pct Recovery = 74% Analysis Date = 06/12/15 Pct Recovery = 74% Analysis Date = 06/03/15 Pct Recovery = 74% Analysis Date = 06/03/15 Pct Recovery = 74% Analysis Date = 05/25/15 Pct Recovery = 74% Analysis Date = 05/25/15 Pct Recovery = 74% Analysis Date = 05/16/15 Pct Recovery = 73% Analysis Date = 05/16/15 Pct Recovery = 73% Analysis Date = 05/06/15 Pct Recovery = 73% Analysis Date = 05/06/15 Pct Recovery = 73% Analysis Date = 04/27/15 Pct Recovery = 73% Analysis Date = 04/27/15 Pct Recovery = 73% Analysis Date = 04/18/15 Pct Recovery = 73% Analysis Date = 04/18/15 Pct Recovery = 73% Analysis Date = 04/09/15 Pct Recovery = 73% Analysis Date = 04/09/15 Pct Recovery = 73% Analysis Date = 03/30/15 Pct Recovery = 73% Analysis Date = 03/30/15 Pct Recovery = 73% Analysis Date = 03/21/15 Pct Recovery = 73% Analysis Date = 03/21/15 Pct Recovery = 73% Analysis Date = 03/12/15 Pct Recovery = 73% Analysis Date = 03/12/15 Pct Recovery = 73% Analysis Date = 03/03/15 Pct Recovery = 73% Analysis Date = 03/03/15 Pct Recovery = 73% Analysis Date = 02/21/15 Pct Recovery = 73% Analysis Date = 02/21/15 Pct Recovery = 73% Analysis Date = 02/12/15 Pct Recovery = 73% Analysis Date = 02/12/15 Pct Recovery = 73% Analysis Date = 02/03/15 Pct Recovery = 73% Analysis Date = 02/03/15 Pct Recovery = 73% Analysis Date = 01/25/15 Pct Recovery = 73% Analysis Date = 01/25/15 Pct Recovery = 73% Analysis Date = 01/15/15 Pct Recovery = 73% Analysis Date = 01/15/15 Pct Recovery = 73% Analysis Date = 01/06/15 Pct Recovery = 73% Analysis Date = 01/06/15 Pct Recovery = 73% Analysis Date = 12/28/14 Pct Recovery = 73% Analysis Date = 12/28/14 Pct Recovery = 73% Analysis Date = 12/19/14 Pct Recovery = 73% Analysis Date = 12/19/14 Pct Recovery = 73% Analysis Date = 12/09/14 Pct Recovery = 73% Analysis Date = 12/09/14 Pct Recovery = 73% Analysis Date = 11/30/14 Pct Recovery = 73% Analysis Date = 11/30/14 Pct Recovery = 73% Analysis Date = 11/21/14 Pct Recovery = 73% Analysis Date = 11/21/14 Pct Recovery = 73% Analysis Date = 11/12/14 Pct Recovery = 73% Analysis Date = 11/12/14 Pct Recovery = 73% Analysis Date = 11/02/14 Pct Recovery = 73% Analysis Date = 11/02/14 Pct Recovery = 73% Analysis Date = 10/24/14 Pct Recovery = 73% Analysis Date = 10/24/14 Pct Recovery = 73% Analysis Date = 10/15/14 Pct Recovery = 73% Analysis Date = 10/15/14 Pct Recovery = 73% Analysis Date = 10/06/14 Pct Recovery = 73% Analysis Date = 10/06/14 Pct Recovery = 73% Analysis Date = 09/26/14 Pct Recovery = 73% Analysis Date = 09/26/14 Pct Recovery = 73% Analysis Date = 09/17/14 Pct Recovery = 73% Analysis Date = 09/17/14 Pct Recovery = 73% Analysis Date = 09/08/14 Pct Recovery = 74% Analysis Date = 09/08/14 Pct Recovery = 74% Analysis Date = 08/30/14 Pct Recovery = 74% Analysis Date = 08/30/14 Pct Recovery = 74% Analysis Date = 08/20/14 Pct Recovery = 74% Analysis Date = 08/20/14 Pct Recovery = 74% Analysis Date = 08/11/14 Pct Recovery = 74% Analysis Date = 08/11/14 Pct Recovery = 74% Analysis Date = 08/02/14 Pct Recovery = 74% Analysis Date = 08/02/14 Pct Recovery = 74% Analysis Date = 07/24/14 Pct Recovery = 74% Analysis Date = 07/24/14 Pct Recovery = 74% Analysis Date = 07/14/14 Pct Recovery = 74% Analysis Date = 07/14/14 Pct Recovery = 74% Analysis Date = 07/05/14 Pct Recovery = 74% Analysis Date = 07/05/14 Pct Recovery = 74% Analysis Date = 06/26/14 Pct Recovery = 75% Analysis Date = 06/26/14 Pct Recovery = 75% Analysis Date = 06/17/14 Pct Recovery = 75% Analysis Date = 06/17/14 Pct Recovery = 75% Analysis Date = 06/07/14 Pct Recovery = 75% Analysis Date = 06/07/14 Pct Recovery = 75% Analysis Date = 05/29/14 Pct Recovery = 75% Analysis Date = 05/29/14 Pct Recovery = 75% Analysis Date = 05/20/14 Pct Recovery = 75% Analysis Date = 05/20/14 Pct Recovery = 75% Analysis Date = 05/11/14 Pct Recovery = 76% Analysis Date = 05/11/14 Pct Recovery = 76% Analysis Date = 05/01/14 Pct Recovery = 76% Analysis Date = 05/01/14 Pct Recovery = 76% Analysis Date = 04/22/14 Pct Recovery = 76% Analysis Date = 04/22/14 Pct Recovery = 76% Analysis Date = 04/13/14 Pct Recovery = 76% Analysis Date = 04/13/14 Pct Recovery = 76% Analysis Date = 04/04/14 Pct Recovery = 76% Analysis Date = 04/04/14 Pct Recovery = 76% Analysis Date = 03/25/14 Pct Recovery = 77% Analysis Date = 03/25/14 Pct Recovery = 77% Analysis Date = 03/16/14 Pct Recovery = 77% Analysis Date = 03/16/14 Pct Recovery = 77% Analysis Date = 03/07/14 Pct Recovery = 77% Analysis Date = 03/07/14 Pct Recovery = 77% Analysis Date = 02/26/14 Pct Recovery = 77% Analysis Date = 02/26/14 Pct Recovery = 77% Analysis Date = 02/16/14 Pct Recovery = 78% Analysis Date = 02/16/14 Pct Recovery = 78% Analysis Date = 02/07/14 Pct Recovery = 78% Analysis Date = 02/07/14 Pct Recovery = 78% Analysis Date = 01/29/14 Pct Recovery = 78% Analysis Date = 01/29/14 Pct Recovery = 78% Analysis Date = 01/20/14 Pct Recovery = 78% Analysis Date = 01/20/14 Pct Recovery = 78% Analysis Date = 01/10/14 Pct Recovery = 78% Analysis Date = 01/10/14 Pct Recovery = 78% Analysis Date = 01/01/14 Pct Recovery = 79% Analysis Date = 01/01/14 Pct Recovery = 79% Analysis Date = 12/23/13 Pct Recovery = 79% Analysis Date = 12/23/13 Pct Recovery = 79% Analysis Date = 12/14/13 Pct Recovery = 79% Analysis Date = 12/14/13 Pct Recovery = 79% Analysis Date = 12/04/13 Pct Recovery = 79% Analysis Date = 12/04/13 Pct Recovery = 79% Analysis Date = 11/25/13 Pct Recovery = 80% Analysis Date = 11/25/13 Pct Recovery = 80% Analysis Date = 11/16/13 Pct Recovery = 80% Analysis Date = 11/16/13 Pct Recovery = 80% Analysis Date = 11/07/13 Pct Recovery = 80% Analysis Date = 11/07/13 Pct Recovery = 80% Analysis Date = 10/28/13 Pct Recovery = 80% Analysis Date = 10/28/13 Pct Recovery = 80% Analysis Date = 10/19/13 Pct Recovery = 80% Analysis Date = 10/19/13 Pct Recovery = 80% Analysis Date = 10/10/13 Pct Recovery = 81% Analysis Date = 10/10/13 Pct Recovery = 81% Analysis Date = 10/01/13 Pct Recovery = 81% Analysis Date = 10/01/13 Pct Recovery = 81% Analysis Date = 09/21/13 Pct Recovery = 81% Analysis Date = 09/21/13 Pct Recovery = 81% Analysis Date = 09/12/13 Pct Recovery = 81% Analysis Date = 09/12/13 Pct Recovery = 81% Analysis Date = 09/03/13 Pct Recovery = 82% Analysis Date = 09/03/13 Pct Recovery = 82% Analysis Date = 08/25/13 Pct Recovery = 82% Analysis Date = 08/25/13 Pct Recovery = 82% Analysis Date = 08/15/13 Pct Recovery = 82% Analysis Date = 08/15/13 Pct Recovery = 82% Analysis Date = 08/06/13 Pct Recovery = 82% Analysis Date = 08/06/13 Pct Recovery = 82% Analysis Date = 07/28/13 Pct Recovery = 83% Analysis Date = 07/28/13 Pct Recovery = 83% Analysis Date = 07/19/13 Pct Recovery = 83% Analysis Date = 07/19/13 Pct Recovery = 83% Analysis Date = 07/09/13 Pct Recovery = 83% Analysis Date = 07/09/13 Pct Recovery = 83% Analysis Date = 06/30/13 Pct Recovery = 83% Analysis Date = 06/30/13 Pct Recovery = 83% Analysis Date = 06/21/13 Pct Recovery = 84% Analysis Date = 06/21/13 Pct Recovery = 84% Analysis Date = 06/12/13 Pct Recovery = 84% Analysis Date = 06/12/13 Pct Recovery = 84% Analysis Date = 06/02/13 Pct Recovery = 84% Analysis Date = 06/02/13 Pct Recovery = 84% Analysis Date = 05/24/13 Pct Recovery = 84% Analysis Date = 05/24/13 Pct Recovery = 84% Analysis Date = 05/15/13 Pct Recovery = 85% Analysis Date = 05/15/13 Pct Recovery = 85% Analysis Date = 05/06/13 Pct Recovery = 85% Analysis Date = 05/06/13 Pct Recovery = 85% Analysis Date = 04/26/13 Pct Recovery = 85% Analysis Date = 04/26/13 Pct Recovery = 85% Analysis Date = 04/17/13 Pct Recovery = 85% Analysis Date = 04/17/13 Pct Recovery = 85% Analysis Date = 04/08/13 Pct Recovery = 86% Analysis Date = 04/08/13 Pct Recovery = 86% Analysis Date = 03/30/13 Pct Recovery = 86% Analysis Date = 03/30/13 Pct Recovery = 86% Analysis Date = 03/20/13 Pct Recovery = 86% Analysis Date = 03/20/13 Pct Recovery = 86% Analysis Date = 03/11/13 Pct Recovery = 86% Analysis Date = 03/11/13 Pct Recovery = 86% Analysis Date = 03/02/13 Pct Recovery = 87% Analysis Date = 03/02/13 Pct Recovery = 87% Analysis Date = 02/21/13 Pct Recovery = 87% Analysis Date = 02/21/13 Pct Recovery = 87% Analysis Date = 02/11/13 Pct Recovery = 87% Analysis Date = 02/11/13 Pct Recovery = 87% Analysis Date = 02/02/13 Pct Recovery = 87% Analysis Date = 02/02/13 Pct Recovery = 87% Analysis Date = 01/24/13 Pct Recovery = 88% Analysis Date = 01/24/13 Pct Recovery = 88% Analysis Date = 01/15/13 Pct Recovery = 88% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
ENDOSULFAN SULFATE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 72 80% 14% 77% 12%
Total 72 80% 14% 77% 12%

Sample Statistics
ENDOSULFAN SULFATE

Characteristic N % % Basis
Plotted 72 100% Spiked
Estimated Values 1 1% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 72 .  
False Negatives 0 0% 0 out of 72
Not Spiked 46 .  
False Positives 0 0% 0 out of 46

OBSP Determination:
EPTC
METHOD: 2033 , TESTIDCODE: 82668GCM35

Laboratory ID = 20130250061 Lab Value = 0.137 Expected Conc. = 0.15 Report level label = 0.0056 Pct Recovery = 91% Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl SpecificMix = A088380 Laboratory ID = 20140230082 Lab Value = 0.066 Expected Conc. = 0.075 Report level label = 0.0056 Pct Recovery = 88% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl SpecificMix = A093651 Laboratory ID = 20132420001 Lab Value = 0.070 Expected Conc. = 0.075 Report level label = 0.0056 Pct Recovery = 93% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl SpecificMix = A093651 Laboratory ID = 20130810108 Lab Value = 0.072 Expected Conc. = 0.075 Report level label = 0.0056 Pct Recovery = 96% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl SpecificMix = T1120530013 Laboratory ID = 20123560092 Lab Value = 0.067 Expected Conc. = 0.075 Report level label = 0.0056 Pct Recovery = 89% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = T1120530013 Laboratory ID = 20140100085 Lab Value = 0.049 Expected Conc. = 0.05 Report level label = 0.0056 Pct Recovery = 97% Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl SpecificMix = T1130514013 Laboratory ID = 20132490342 Lab Value = 0.049 Expected Conc. = 0.05 Report level label = 0.0056 Pct Recovery = 99% Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl SpecificMix = T1130514013 Laboratory ID = 20180390003 Lab Value = 0.039 Expected Conc. = 0.038 Report level label = 0.008 Pct Recovery = 103% Analysis Date = 04/06/18 SpikeMix = Spex Organics EN170808006: 100 µl & Abs 071717Pest: 100 µl SpecificMix = 071717Pest Laboratory ID = 20172510330 Lab Value = 0.034 Expected Conc. = 0.037 Report level label = 0.0056 Pct Recovery = 92% Analysis Date = 12/29/17 SpikeMix = ChemService 6537100: 100 µl & Abs 071817Pest: 100 µl SpecificMix = 6537100 Laboratory ID = 20162860079 Lab Value = 0.042 Expected Conc. = 0.035 Report level label = 0.0056 Pct Recovery = 121% Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl SpecificMix = 060916 Laboratory ID = 20163150006 Lab Value = 0.038 Expected Conc. = 0.035 Report level label = 0.0056 Pct Recovery = 107% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl SpecificMix = 060916 Laboratory ID = 20152750006 Lab Value = 0.018 Expected Conc. = 0.0336 Report level label = 0.0056 Pct Recovery = 53% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl SpecificMix = 040615 Laboratory ID = 20152610011 Lab Value = 0.033 Expected Conc. = 0.0336 Report level label = 0.0056 Pct Recovery = 99% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl SpecificMix = 040615 Laboratory ID = 20140860102 Lab Value = 0.025 Expected Conc. = 0.03 Report level label = 0.0056 Pct Recovery = 85% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl SpecificMix = A093651 Laboratory ID = 20133400002 Lab Value = 0.031 Expected Conc. = 0.03 Report level label = 0.0056 Pct Recovery = 102% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = A093651 Laboratory ID = 20132910008 Lab Value = 0.029 Expected Conc. = 0.03 Report level label = 0.0056 Pct Recovery = 95% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = A093651 Laboratory ID = 20131920149 Lab Value = 0.029 Expected Conc. = 0.03 Report level label = 0.0056 Pct Recovery = 97% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl SpecificMix = A093651 Laboratory ID = 20131230084 Lab Value = 0.031 Expected Conc. = 0.03 Report level label = 0.0056 Pct Recovery = 102% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl SpecificMix = A088380 Laboratory ID = 20130650005 Lab Value = 0.025 Expected Conc. = 0.03 Report level label = 0.0056 Pct Recovery = 82% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl SpecificMix = A088380 Laboratory ID = 20130390105 Lab Value = 0.026 Expected Conc. = 0.03 Report level label = 0.0056 Pct Recovery = 87% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl SpecificMix = T1120530013 Laboratory ID = 20171660002 Lab Value = 0.031 Expected Conc. = 0.028 Report level label = 0.0056 Pct Recovery = 109% Analysis Date = 08/23/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = 060916 Laboratory ID = 20171380001 Lab Value = 0.024 Expected Conc. = 0.028 Report level label = 0.0056 Pct Recovery = 84% Analysis Date = 06/07/17 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 041816 Laboratory ID = 20170740063 Lab Value = 0.027 Expected Conc. = 0.028 Report level label = 0.0056 Pct Recovery = 97% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl SpecificMix = 041816 Laboratory ID = 20170190026 Lab Value = 0.028 Expected Conc. = 0.028 Report level label = 0.0056 Pct Recovery = 100% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = 060916 Laboratory ID = 20161740258 Lab Value = 0.022 Expected Conc. = 0.028 Report level label = 0.0056 Pct Recovery = 80% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 041816 Laboratory ID = 20140370077 Lab Value = 0.021 Expected Conc. = 0.025 Report level label = 0.0056 Pct Recovery = 83% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl SpecificMix = T1130514013 Laboratory ID = 20132690010 Lab Value = 0.026 Expected Conc. = 0.025 Report level label = 0.0056 Pct Recovery = 105% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl SpecificMix = T1130514013 Laboratory ID = 20131370001 Lab Value = 0.028 Expected Conc. = 0.025 Report level label = 0.0056 Pct Recovery = 113% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl SpecificMix = 1473000 Laboratory ID = 20142720002 Lab Value = 0.021 Expected Conc. = 0.0223 Report level label = 0.0056 Pct Recovery = 93% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl SpecificMix = LC06435 Laboratory ID = 20142530087 Lab Value = 0.020 Expected Conc. = 0.0223 Report level label = 0.0056 Pct Recovery = 89% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl SpecificMix = LC06435 Laboratory ID = 20141570088 Lab Value = 0.023 Expected Conc. = 0.0223 Report level label = 0.0056 Pct Recovery = 102% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl SpecificMix = LC06435 Laboratory ID = 20141220025 Lab Value = 0.021 Expected Conc. = 0.0223 Report level label = 0.0056 Pct Recovery = 93% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl SpecificMix = LC06435 Laboratory ID = 20150720069 Lab Value = 0.024 Expected Conc. = 0.0222 Report level label = 0.0056 Pct Recovery = 106% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 03DD006 Laboratory ID = 20143110108 Lab Value = 0.020 Expected Conc. = 0.0222 Report level label = 0.0056 Pct Recovery = 89% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 03DD006 Laboratory ID = 20142960086 Lab Value = 0.020 Expected Conc. = 0.0222 Report level label = 0.0056 Pct Recovery = 91% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 03DD006 Laboratory ID = 20142270001 Lab Value = 0.021 Expected Conc. = 0.0222 Report level label = 0.0056 Pct Recovery = 93% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl SpecificMix = 03DD006 Laboratory ID = 20173480003 Lab Value = 0.020 Expected Conc. = 0.019 Report level label = 0.008 Pct Recovery = 105% Analysis Date = 04/05/18 SpikeMix = Abs 071717Pest: 50 µl & ChemService 6567600: 50 µl SpecificMix = 071717Pest Laboratory ID = 20172230001 Lab Value = 0.024 Expected Conc. = 0.019 Report level label = 0.0056 Pct Recovery = 126% Analysis Date = 10/19/17 SpikeMix = ChemService 6472100: 50 µl & Abs 071717Pest: 50 µl SpecificMix = 071717Pest Laboratory ID = 20172370001 Lab Value = 0.019 Expected Conc. = 0.0185 Report level label = 0.0056 Pct Recovery = 105% Analysis Date = 11/18/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6537100: 50 µl SpecificMix = 6537100 Laboratory ID = 20161260151 Lab Value = 0.017 Expected Conc. = 0.0168 Report level label = 0.0056 Pct Recovery = 98% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = EN150513008 Laboratory ID = 20160770090 Lab Value = 0.016 Expected Conc. = 0.0168 Report level label = 0.0056 Pct Recovery = 97% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = EN150513008 Laboratory ID = 20153510109 Lab Value = 0.014 Expected Conc. = 0.0168 Report level label = 0.0056 Pct Recovery = 85% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = EN150513008 Laboratory ID = 20152330039 Lab Value = 0.013 Expected Conc. = 0.0168 Report level label = 0.0056 Pct Recovery = 79% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl SpecificMix = EN150513008 Laboratory ID = 20151900132 Lab Value = 0.013 Expected Conc. = 0.0168 Report level label = 0.0056 Pct Recovery = 76% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl SpecificMix = 040615 Laboratory ID = 20151550293 Lab Value = 0.017 Expected Conc. = 0.0168 Report level label = 0.0056 Pct Recovery = 102% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl SpecificMix = 040615 Laboratory ID = 20172020035 Lab Value = 0.019 Expected Conc. = 0.0152 Report level label = 0.0056 Pct Recovery = 122% Analysis Date = 11/07/17 SpikeMix = Abs 071717Pest: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 071717Pest Laboratory ID = 20171940002 Lab Value = 0.015 Expected Conc. = 0.014 Report level label = 0.0056 Pct Recovery = 106% Analysis Date = 11/10/17 SpikeMix = ChemService 5054800: 40 µl & NSI 041816: 40 µl SpecificMix = 041816 Laboratory ID = 20171160110 Lab Value = 0.015 Expected Conc. = 0.014 Report level label = 0.0056 Pct Recovery = 105% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = 060916 Laboratory ID = 20162520001 Lab Value = 0.019 Expected Conc. = 0.014 Report level label = 0.0056 Pct Recovery = 137% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl SpecificMix = 060916 Laboratory ID = 20163560019 Lab Value = 0.015 Expected Conc. = 0.014 Report level label = 0.0056 Pct Recovery = 110% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl SpecificMix = 060916 Laboratory ID = 20162380004 Lab Value = 0.016 Expected Conc. = 0.014 Report level label = 0.0056 Pct Recovery = 112% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = 060916 Laboratory ID = 20162020124 Lab Value = 0.015 Expected Conc. = 0.014 Report level label = 0.0056 Pct Recovery = 104% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl SpecificMix = 041816 Laboratory ID = 20161600087 Lab Value = 0.014 Expected Conc. = 0.014 Report level label = 0.0056 Pct Recovery = 96% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 041816 Laboratory ID = 20161340228 Lab Value = 0.011 Expected Conc. = 0.014 Report level label = 0.0056 Pct Recovery = 81% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl SpecificMix = 041816 Laboratory ID = 20161190075 Lab Value = 0.012 Expected Conc. = 0.014 Report level label = 0.0056 Pct Recovery = 85% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 041816 Laboratory ID = 20180940080 Lab Value = 0.012 Expected Conc. = 0.0114 Report level label = 0.008 Pct Recovery = 105% Analysis Date = 05/31/18 SpikeMix = ChemService 6472100: 30 µl & Abs 071717Pest: 30 µl SpecificMix = 071717Pest Laboratory ID = 20180730064 Lab Value = 0.015 Expected Conc. = 0.0114 Report level label = 0.008 Pct Recovery = 132% Analysis Date = 05/16/18 SpikeMix = Abs 071717Pest: 30 µl & Abs 071817Pest: 30 µl SpecificMix = 071717Pest Laboratory ID = 20150150115 Lab Value = 0.011 Expected Conc. = 0.0112 Report level label = 0.0056 Pct Recovery = 94% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl SpecificMix = LC06435 Laboratory ID = 20143370094 Lab Value = 0.010 Expected Conc. = 0.0112 Report level label = 0.0056 Pct Recovery = 88% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl SpecificMix = LC06435 Laboratory ID = 20141910243 Lab Value = 0.011 Expected Conc. = 0.0112 Report level label = 0.0056 Pct Recovery = 94% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = LC06435 Laboratory ID = 20141840097 Lab Value = 0.011 Expected Conc. = 0.0112 Report level label = 0.0056 Pct Recovery = 101% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl SpecificMix = LC06435 Laboratory ID = 20173120093 Lab Value = 0.013 Expected Conc. = 0.0111 Report level label = 0.0056 Pct Recovery = 114% Analysis Date = 03/10/18 SpikeMix = ChemService 6472100: 30 µl & ChemService 6537100: 30 µl SpecificMix = 6537100 Laboratory ID = 20172780018 Lab Value = 0.011 Expected Conc. = 0.0111 Report level label = 0.0056 Pct Recovery = 95% Analysis Date = 02/08/18 SpikeMix = ChemService 6537100: 30 µl & Abs 071817Pest: 30 µl SpecificMix = 6537100 Laboratory ID = 20142200164 Lab Value = 0.011 Expected Conc. = 0.0111 Report level label = 0.0056 Pct Recovery = 103% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 03DD006 Laboratory ID = 20141640076 Lab Value = 0.011 Expected Conc. = 0.0111 Report level label = 0.0056 Pct Recovery = 102% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = 03DD006 Laboratory ID = 20141420140 Lab Value = 0.012 Expected Conc. = 0.0111 Report level label = 0.0056 Pct Recovery = 105% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 03DD006 Laboratory ID = 20141080004 Lab Value = 0.013 Expected Conc. = 0.0111 Report level label = 0.0056 Pct Recovery = 114% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl SpecificMix = 03DD006 Laboratory ID = 20140730138 Lab Value = 0.010 Expected Conc. = 0.01 Report level label = 0.0056 Pct Recovery = 104% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 1473000 Laboratory ID = 20133470008 Lab Value = 0.010 Expected Conc. = 0.01 Report level label = 0.0056 Pct Recovery = 104% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl SpecificMix = 1473000 Laboratory ID = 20133310030 Lab Value = 0.011 Expected Conc. = 0.01 Report level label = 0.0056 Pct Recovery = 110% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl SpecificMix = 1473000 Laboratory ID = 20133050050 Lab Value = 0.011 Expected Conc. = 0.01 Report level label = 0.0056 Pct Recovery = 108% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl SpecificMix = T1130514013 Laboratory ID = 20132280016 Lab Value = 0.011 Expected Conc. = 0.01 Report level label = 0.0056 Pct Recovery = 112% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl SpecificMix = T1130514013 Laboratory ID = 20131790009 Lab Value = 0.010 Expected Conc. = 0.01 Report level label = 0.0056 Pct Recovery = 99% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl SpecificMix = 1473000 Laboratory ID = 20131650073 Lab Value = 0.010 Expected Conc. = 0.01 Report level label = 0.0056 Pct Recovery = 98% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl SpecificMix = 1473000 Laboratory ID = 20161050143 Lab Value = 0.009 Expected Conc. = 0.0084 Report level label = 0.0056 Pct Recovery = 108% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Laboratory ID = 20160430111 Lab Value = 0.009 Expected Conc. = 0.0084 Report level label = 0.0056 Pct Recovery = 112% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Laboratory ID = 20160560044 Lab Value = 0.008 Expected Conc. = 0.0084 Report level label = 0.0056 Pct Recovery = 98% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl SpecificMix = EN150513008 Laboratory ID = 20160070059 Lab Value = 0.009 Expected Conc. = 0.0084 Report level label = 0.0056 Pct Recovery = 101% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = 040615 Laboratory ID = 20153160001 Lab Value = 0.009 Expected Conc. = 0.0084 Report level label = 0.0056 Pct Recovery = 105% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = EN150513008 Laboratory ID = 20153030068 Lab Value = 0.009 Expected Conc. = 0.0084 Report level label = 0.0056 Pct Recovery = 110% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150513008 Laboratory ID = 20152190003 Lab Value = 0.005 Expected Conc. = 0.0084 Report level label = 0.0056 Pct Recovery = 55% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150513008 Laboratory ID = 20151480170 Lab Value = 0.009 Expected Conc. = 0.0084 Report level label = 0.0056 Pct Recovery = 105% Analysis Date = 06/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150513008 Laboratory ID = 20151380009 Lab Value = 0.008 Expected Conc. = 0.0084 Report level label = 0.0056 Pct Recovery = 89% Analysis Date = 05/30/15 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Laboratory ID = 20151210037 Lab Value = 0.009 Expected Conc. = 0.0084 Report level label = 0.0056 Pct Recovery = 108% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Analysis Date = 05/31/18 Pct Recovery = 113% Analysis Date = 05/21/18 Pct Recovery = 113% Analysis Date = 05/21/18 Pct Recovery = 113% Analysis Date = 05/11/18 Pct Recovery = 113% Analysis Date = 05/11/18 Pct Recovery = 113% Analysis Date = 05/01/18 Pct Recovery = 112% Analysis Date = 05/01/18 Pct Recovery = 112% Analysis Date = 04/21/18 Pct Recovery = 112% Analysis Date = 04/21/18 Pct Recovery = 112% Analysis Date = 04/11/18 Pct Recovery = 112% Analysis Date = 04/11/18 Pct Recovery = 112% Analysis Date = 04/02/18 Pct Recovery = 112% Analysis Date = 04/02/18 Pct Recovery = 112% Analysis Date = 03/23/18 Pct Recovery = 112% Analysis Date = 03/23/18 Pct Recovery = 112% Analysis Date = 03/13/18 Pct Recovery = 111% Analysis Date = 03/13/18 Pct Recovery = 111% Analysis Date = 03/03/18 Pct Recovery = 111% Analysis Date = 03/03/18 Pct Recovery = 111% Analysis Date = 02/21/18 Pct Recovery = 111% Analysis Date = 02/21/18 Pct Recovery = 111% Analysis Date = 02/12/18 Pct Recovery = 111% Analysis Date = 02/12/18 Pct Recovery = 111% Analysis Date = 02/02/18 Pct Recovery = 111% Analysis Date = 02/02/18 Pct Recovery = 111% Analysis Date = 01/23/18 Pct Recovery = 110% Analysis Date = 01/23/18 Pct Recovery = 110% Analysis Date = 01/13/18 Pct Recovery = 110% Analysis Date = 01/13/18 Pct Recovery = 110% Analysis Date = 01/03/18 Pct Recovery = 110% Analysis Date = 01/03/18 Pct Recovery = 110% Analysis Date = 12/25/17 Pct Recovery = 110% Analysis Date = 12/25/17 Pct Recovery = 110% Analysis Date = 12/15/17 Pct Recovery = 110% Analysis Date = 12/15/17 Pct Recovery = 110% Analysis Date = 12/05/17 Pct Recovery = 109% Analysis Date = 12/05/17 Pct Recovery = 109% Analysis Date = 11/25/17 Pct Recovery = 109% Analysis Date = 11/25/17 Pct Recovery = 109% Analysis Date = 11/15/17 Pct Recovery = 109% Analysis Date = 11/15/17 Pct Recovery = 109% Analysis Date = 11/05/17 Pct Recovery = 109% Analysis Date = 11/05/17 Pct Recovery = 109% Analysis Date = 10/27/17 Pct Recovery = 109% Analysis Date = 10/27/17 Pct Recovery = 109% Analysis Date = 10/17/17 Pct Recovery = 108% Analysis Date = 10/17/17 Pct Recovery = 108% Analysis Date = 10/07/17 Pct Recovery = 108% Analysis Date = 10/07/17 Pct Recovery = 108% Analysis Date = 09/27/17 Pct Recovery = 108% Analysis Date = 09/27/17 Pct Recovery = 108% Analysis Date = 09/17/17 Pct Recovery = 108% Analysis Date = 09/17/17 Pct Recovery = 108% Analysis Date = 09/08/17 Pct Recovery = 107% Analysis Date = 09/08/17 Pct Recovery = 107% Analysis Date = 08/29/17 Pct Recovery = 107% Analysis Date = 08/29/17 Pct Recovery = 107% Analysis Date = 08/19/17 Pct Recovery = 107% Analysis Date = 08/19/17 Pct Recovery = 107% Analysis Date = 08/09/17 Pct Recovery = 107% Analysis Date = 08/09/17 Pct Recovery = 107% Analysis Date = 07/30/17 Pct Recovery = 107% Analysis Date = 07/30/17 Pct Recovery = 107% Analysis Date = 07/21/17 Pct Recovery = 106% Analysis Date = 07/21/17 Pct Recovery = 106% Analysis Date = 07/11/17 Pct Recovery = 106% Analysis Date = 07/11/17 Pct Recovery = 106% Analysis Date = 07/01/17 Pct Recovery = 106% Analysis Date = 07/01/17 Pct Recovery = 106% Analysis Date = 06/21/17 Pct Recovery = 106% Analysis Date = 06/21/17 Pct Recovery = 106% Analysis Date = 06/11/17 Pct Recovery = 106% Analysis Date = 06/11/17 Pct Recovery = 106% Analysis Date = 06/02/17 Pct Recovery = 105% Analysis Date = 06/02/17 Pct Recovery = 105% Analysis Date = 05/23/17 Pct Recovery = 105% Analysis Date = 05/23/17 Pct Recovery = 105% Analysis Date = 05/13/17 Pct Recovery = 105% Analysis Date = 05/13/17 Pct Recovery = 105% Analysis Date = 05/03/17 Pct Recovery = 105% Analysis Date = 05/03/17 Pct Recovery = 105% Analysis Date = 04/23/17 Pct Recovery = 104% Analysis Date = 04/23/17 Pct Recovery = 104% Analysis Date = 04/13/17 Pct Recovery = 104% Analysis Date = 04/13/17 Pct Recovery = 104% Analysis Date = 04/04/17 Pct Recovery = 104% Analysis Date = 04/04/17 Pct Recovery = 104% Analysis Date = 03/25/17 Pct Recovery = 104% Analysis Date = 03/25/17 Pct Recovery = 104% Analysis Date = 03/15/17 Pct Recovery = 104% Analysis Date = 03/15/17 Pct Recovery = 104% Analysis Date = 03/05/17 Pct Recovery = 103% Analysis Date = 03/05/17 Pct Recovery = 103% Analysis Date = 02/23/17 Pct Recovery = 103% Analysis Date = 02/23/17 Pct Recovery = 103% Analysis Date = 02/14/17 Pct Recovery = 103% Analysis Date = 02/14/17 Pct Recovery = 103% Analysis Date = 02/04/17 Pct Recovery = 103% Analysis Date = 02/04/17 Pct Recovery = 103% Analysis Date = 01/25/17 Pct Recovery = 103% Analysis Date = 01/25/17 Pct Recovery = 103% Analysis Date = 01/15/17 Pct Recovery = 102% Analysis Date = 01/15/17 Pct Recovery = 102% Analysis Date = 01/05/17 Pct Recovery = 102% Analysis Date = 01/05/17 Pct Recovery = 102% Analysis Date = 12/27/16 Pct Recovery = 102% Analysis Date = 12/27/16 Pct Recovery = 102% Analysis Date = 12/17/16 Pct Recovery = 102% Analysis Date = 12/17/16 Pct Recovery = 102% Analysis Date = 12/07/16 Pct Recovery = 102% Analysis Date = 12/07/16 Pct Recovery = 102% Analysis Date = 11/27/16 Pct Recovery = 101% Analysis Date = 11/27/16 Pct Recovery = 101% Analysis Date = 11/17/16 Pct Recovery = 101% Analysis Date = 11/17/16 Pct Recovery = 101% Analysis Date = 11/08/16 Pct Recovery = 101% Analysis Date = 11/08/16 Pct Recovery = 101% Analysis Date = 10/29/16 Pct Recovery = 101% Analysis Date = 10/29/16 Pct Recovery = 101% Analysis Date = 10/19/16 Pct Recovery = 101% Analysis Date = 10/19/16 Pct Recovery = 101% Analysis Date = 10/09/16 Pct Recovery = 100% Analysis Date = 10/09/16 Pct Recovery = 100% Analysis Date = 09/29/16 Pct Recovery = 100% Analysis Date = 09/29/16 Pct Recovery = 100% Analysis Date = 09/19/16 Pct Recovery = 100% Analysis Date = 09/19/16 Pct Recovery = 100% Analysis Date = 09/10/16 Pct Recovery = 100% Analysis Date = 09/10/16 Pct Recovery = 100% Analysis Date = 08/31/16 Pct Recovery = 100% Analysis Date = 08/31/16 Pct Recovery = 100% Analysis Date = 08/21/16 Pct Recovery = 99% Analysis Date = 08/21/16 Pct Recovery = 99% Analysis Date = 08/11/16 Pct Recovery = 99% Analysis Date = 08/11/16 Pct Recovery = 99% Analysis Date = 08/01/16 Pct Recovery = 99% Analysis Date = 08/01/16 Pct Recovery = 99% Analysis Date = 07/23/16 Pct Recovery = 99% Analysis Date = 07/23/16 Pct Recovery = 99% Analysis Date = 07/13/16 Pct Recovery = 98% Analysis Date = 07/13/16 Pct Recovery = 98% Analysis Date = 07/03/16 Pct Recovery = 98% Analysis Date = 07/03/16 Pct Recovery = 98% Analysis Date = 06/23/16 Pct Recovery = 98% Analysis Date = 06/23/16 Pct Recovery = 98% Analysis Date = 06/13/16 Pct Recovery = 98% Analysis Date = 06/13/16 Pct Recovery = 98% Analysis Date = 06/04/16 Pct Recovery = 98% Analysis Date = 06/04/16 Pct Recovery = 98% Analysis Date = 05/25/16 Pct Recovery = 97% Analysis Date = 05/25/16 Pct Recovery = 97% Analysis Date = 05/15/16 Pct Recovery = 97% Analysis Date = 05/15/16 Pct Recovery = 97% Analysis Date = 05/05/16 Pct Recovery = 97% Analysis Date = 05/05/16 Pct Recovery = 97% Analysis Date = 04/25/16 Pct Recovery = 97% Analysis Date = 04/25/16 Pct Recovery = 97% Analysis Date = 04/16/16 Pct Recovery = 97% Analysis Date = 04/16/16 Pct Recovery = 97% Analysis Date = 04/06/16 Pct Recovery = 96% Analysis Date = 04/06/16 Pct Recovery = 96% Analysis Date = 03/27/16 Pct Recovery = 96% Analysis Date = 03/27/16 Pct Recovery = 96% Analysis Date = 03/17/16 Pct Recovery = 96% Analysis Date = 03/17/16 Pct Recovery = 96% Analysis Date = 03/07/16 Pct Recovery = 96% Analysis Date = 03/07/16 Pct Recovery = 96% Analysis Date = 02/26/16 Pct Recovery = 95% Analysis Date = 02/26/16 Pct Recovery = 95% Analysis Date = 02/17/16 Pct Recovery = 95% Analysis Date = 02/17/16 Pct Recovery = 95% Analysis Date = 02/07/16 Pct Recovery = 95% Analysis Date = 02/07/16 Pct Recovery = 95% Analysis Date = 01/28/16 Pct Recovery = 95% Analysis Date = 01/28/16 Pct Recovery = 95% Analysis Date = 01/18/16 Pct Recovery = 95% Analysis Date = 01/18/16 Pct Recovery = 95% Analysis Date = 01/08/16 Pct Recovery = 95% Analysis Date = 01/08/16 Pct Recovery = 95% Analysis Date = 12/30/15 Pct Recovery = 94% Analysis Date = 12/30/15 Pct Recovery = 94% Analysis Date = 12/20/15 Pct Recovery = 94% Analysis Date = 12/20/15 Pct Recovery = 94% Analysis Date = 12/10/15 Pct Recovery = 94% Analysis Date = 12/10/15 Pct Recovery = 94% Analysis Date = 11/30/15 Pct Recovery = 94% Analysis Date = 11/30/15 Pct Recovery = 94% Analysis Date = 11/20/15 Pct Recovery = 94% Analysis Date = 11/20/15 Pct Recovery = 94% Analysis Date = 11/11/15 Pct Recovery = 94% Analysis Date = 11/11/15 Pct Recovery = 94% Analysis Date = 11/01/15 Pct Recovery = 94% Analysis Date = 11/01/15 Pct Recovery = 94% Analysis Date = 10/22/15 Pct Recovery = 94% Analysis Date = 10/22/15 Pct Recovery = 94% Analysis Date = 10/12/15 Pct Recovery = 93% Analysis Date = 10/12/15 Pct Recovery = 93% Analysis Date = 10/02/15 Pct Recovery = 93% Analysis Date = 10/02/15 Pct Recovery = 93% Analysis Date = 09/23/15 Pct Recovery = 93% Analysis Date = 09/23/15 Pct Recovery = 93% Analysis Date = 09/13/15 Pct Recovery = 93% Analysis Date = 09/13/15 Pct Recovery = 93% Analysis Date = 09/03/15 Pct Recovery = 93% Analysis Date = 09/03/15 Pct Recovery = 93% Analysis Date = 08/24/15 Pct Recovery = 93% Analysis Date = 08/24/15 Pct Recovery = 93% Analysis Date = 08/14/15 Pct Recovery = 93% Analysis Date = 08/14/15 Pct Recovery = 93% Analysis Date = 08/04/15 Pct Recovery = 93% Analysis Date = 08/04/15 Pct Recovery = 93% Analysis Date = 07/26/15 Pct Recovery = 93% Analysis Date = 07/26/15 Pct Recovery = 93% Analysis Date = 07/16/15 Pct Recovery = 93% Analysis Date = 07/16/15 Pct Recovery = 93% Analysis Date = 07/06/15 Pct Recovery = 93% Analysis Date = 07/06/15 Pct Recovery = 93% Analysis Date = 06/26/15 Pct Recovery = 93% Analysis Date = 06/26/15 Pct Recovery = 93% Analysis Date = 06/16/15 Pct Recovery = 93% Analysis Date = 06/16/15 Pct Recovery = 93% Analysis Date = 06/07/15 Pct Recovery = 93% Analysis Date = 06/07/15 Pct Recovery = 93% Analysis Date = 05/28/15 Pct Recovery = 93% Analysis Date = 05/28/15 Pct Recovery = 93% Analysis Date = 05/18/15 Pct Recovery = 93% Analysis Date = 05/18/15 Pct Recovery = 93% Analysis Date = 05/08/15 Pct Recovery = 94% Analysis Date = 05/08/15 Pct Recovery = 94% Analysis Date = 04/28/15 Pct Recovery = 94% Analysis Date = 04/28/15 Pct Recovery = 94% Analysis Date = 04/19/15 Pct Recovery = 94% Analysis Date = 04/19/15 Pct Recovery = 94% Analysis Date = 04/09/15 Pct Recovery = 94% Analysis Date = 04/09/15 Pct Recovery = 94% Analysis Date = 03/30/15 Pct Recovery = 94% Analysis Date = 03/30/15 Pct Recovery = 94% Analysis Date = 03/20/15 Pct Recovery = 94% Analysis Date = 03/20/15 Pct Recovery = 94% Analysis Date = 03/10/15 Pct Recovery = 94% Analysis Date = 03/10/15 Pct Recovery = 94% Analysis Date = 02/28/15 Pct Recovery = 94% Analysis Date = 02/28/15 Pct Recovery = 94% Analysis Date = 02/19/15 Pct Recovery = 94% Analysis Date = 02/19/15 Pct Recovery = 94% Analysis Date = 02/09/15 Pct Recovery = 94% Analysis Date = 02/09/15 Pct Recovery = 94% Analysis Date = 01/30/15 Pct Recovery = 95% Analysis Date = 01/30/15 Pct Recovery = 95% Analysis Date = 01/20/15 Pct Recovery = 95% Analysis Date = 01/20/15 Pct Recovery = 95% Analysis Date = 01/10/15 Pct Recovery = 95% Analysis Date = 01/10/15 Pct Recovery = 95% Analysis Date = 01/01/15 Pct Recovery = 95% Analysis Date = 01/01/15 Pct Recovery = 95% Analysis Date = 12/22/14 Pct Recovery = 95% Analysis Date = 12/22/14 Pct Recovery = 95% Analysis Date = 12/12/14 Pct Recovery = 95% Analysis Date = 12/12/14 Pct Recovery = 95% Analysis Date = 12/02/14 Pct Recovery = 95% Analysis Date = 12/02/14 Pct Recovery = 95% Analysis Date = 11/22/14 Pct Recovery = 95% Analysis Date = 11/22/14 Pct Recovery = 95% Analysis Date = 11/13/14 Pct Recovery = 95% Analysis Date = 11/13/14 Pct Recovery = 95% Analysis Date = 11/03/14 Pct Recovery = 96% Analysis Date = 11/03/14 Pct Recovery = 96% Analysis Date = 10/24/14 Pct Recovery = 96% Analysis Date = 10/24/14 Pct Recovery = 96% Analysis Date = 10/14/14 Pct Recovery = 96% Analysis Date = 10/14/14 Pct Recovery = 96% Analysis Date = 10/04/14 Pct Recovery = 96% Analysis Date = 10/04/14 Pct Recovery = 96% Analysis Date = 09/25/14 Pct Recovery = 96% Analysis Date = 09/25/14 Pct Recovery = 96% Analysis Date = 09/15/14 Pct Recovery = 96% Analysis Date = 09/15/14 Pct Recovery = 96% Analysis Date = 09/05/14 Pct Recovery = 96% Analysis Date = 09/05/14 Pct Recovery = 96% Analysis Date = 08/26/14 Pct Recovery = 96% Analysis Date = 08/26/14 Pct Recovery = 96% Analysis Date = 08/16/14 Pct Recovery = 96% Analysis Date = 08/16/14 Pct Recovery = 96% Analysis Date = 08/06/14 Pct Recovery = 96% Analysis Date = 08/06/14 Pct Recovery = 96% Analysis Date = 07/28/14 Pct Recovery = 97% Analysis Date = 07/28/14 Pct Recovery = 97% Analysis Date = 07/18/14 Pct Recovery = 97% Analysis Date = 07/18/14 Pct Recovery = 97% Analysis Date = 07/08/14 Pct Recovery = 97% Analysis Date = 07/08/14 Pct Recovery = 97% Analysis Date = 06/28/14 Pct Recovery = 97% Analysis Date = 06/28/14 Pct Recovery = 97% Analysis Date = 06/18/14 Pct Recovery = 97% Analysis Date = 06/18/14 Pct Recovery = 97% Analysis Date = 06/09/14 Pct Recovery = 97% Analysis Date = 06/09/14 Pct Recovery = 97% Analysis Date = 05/30/14 Pct Recovery = 97% Analysis Date = 05/30/14 Pct Recovery = 97% Analysis Date = 05/20/14 Pct Recovery = 97% Analysis Date = 05/20/14 Pct Recovery = 97% Analysis Date = 05/10/14 Pct Recovery = 97% Analysis Date = 05/10/14 Pct Recovery = 97% Analysis Date = 04/30/14 Pct Recovery = 97% Analysis Date = 04/30/14 Pct Recovery = 97% Analysis Date = 04/21/14 Pct Recovery = 97% Analysis Date = 04/21/14 Pct Recovery = 97% Analysis Date = 04/11/14 Pct Recovery = 97% Analysis Date = 04/11/14 Pct Recovery = 97% Analysis Date = 04/01/14 Pct Recovery = 97% Analysis Date = 04/01/14 Pct Recovery = 97% Analysis Date = 03/22/14 Pct Recovery = 97% Analysis Date = 03/22/14 Pct Recovery = 97% Analysis Date = 03/12/14 Pct Recovery = 97% Analysis Date = 03/12/14 Pct Recovery = 97% Analysis Date = 03/03/14 Pct Recovery = 97% Analysis Date = 03/03/14 Pct Recovery = 97% Analysis Date = 02/21/14 Pct Recovery = 97% Analysis Date = 02/21/14 Pct Recovery = 97% Analysis Date = 02/11/14 Pct Recovery = 98% Analysis Date = 02/11/14 Pct Recovery = 98% Analysis Date = 02/01/14 Pct Recovery = 98% Analysis Date = 02/01/14 Pct Recovery = 98% Analysis Date = 01/22/14 Pct Recovery = 98% Analysis Date = 01/22/14 Pct Recovery = 98% Analysis Date = 01/12/14 Pct Recovery = 98% Analysis Date = 01/12/14 Pct Recovery = 98% Analysis Date = 01/03/14 Pct Recovery = 98% Analysis Date = 01/03/14 Pct Recovery = 98% Analysis Date = 12/24/13 Pct Recovery = 98% Analysis Date = 12/24/13 Pct Recovery = 98% Analysis Date = 12/14/13 Pct Recovery = 98% Analysis Date = 12/14/13 Pct Recovery = 98% Analysis Date = 12/04/13 Pct Recovery = 98% Analysis Date = 12/04/13 Pct Recovery = 98% Analysis Date = 11/24/13 Pct Recovery = 98% Analysis Date = 11/24/13 Pct Recovery = 98% Analysis Date = 11/15/13 Pct Recovery = 98% Analysis Date = 11/15/13 Pct Recovery = 98% Analysis Date = 11/05/13 Pct Recovery = 98% Analysis Date = 11/05/13 Pct Recovery = 98% Analysis Date = 10/26/13 Pct Recovery = 98% Analysis Date = 10/26/13 Pct Recovery = 98% Analysis Date = 10/16/13 Pct Recovery = 98% Analysis Date = 10/16/13 Pct Recovery = 98% Analysis Date = 10/06/13 Pct Recovery = 98% Analysis Date = 10/06/13 Pct Recovery = 98% Analysis Date = 09/27/13 Pct Recovery = 98% Analysis Date = 09/27/13 Pct Recovery = 98% Analysis Date = 09/17/13 Pct Recovery = 98% Analysis Date = 09/17/13 Pct Recovery = 98% Analysis Date = 09/07/13 Pct Recovery = 98% Analysis Date = 09/07/13 Pct Recovery = 98% Analysis Date = 08/28/13 Pct Recovery = 98% Analysis Date = 08/28/13 Pct Recovery = 98% Analysis Date = 08/18/13 Pct Recovery = 98% Analysis Date = 08/18/13 Pct Recovery = 98% Analysis Date = 08/09/13 Pct Recovery = 98% Analysis Date = 08/09/13 Pct Recovery = 98% Analysis Date = 07/30/13 Pct Recovery = 98% Analysis Date = 07/30/13 Pct Recovery = 98% Analysis Date = 07/20/13 Pct Recovery = 97% Analysis Date = 07/20/13 Pct Recovery = 97% Analysis Date = 07/10/13 Pct Recovery = 97% Analysis Date = 07/10/13 Pct Recovery = 97% Analysis Date = 06/30/13 Pct Recovery = 97% Analysis Date = 06/30/13 Pct Recovery = 97% Analysis Date = 06/20/13 Pct Recovery = 97% Analysis Date = 06/20/13 Pct Recovery = 97% Analysis Date = 06/11/13 Pct Recovery = 97% Analysis Date = 06/11/13 Pct Recovery = 97% Analysis Date = 06/01/13 Pct Recovery = 97% Analysis Date = 06/01/13 Pct Recovery = 97% Analysis Date = 05/22/13 Pct Recovery = 97% Analysis Date = 05/22/13 Pct Recovery = 97% Analysis Date = 05/12/13 Pct Recovery = 97% Analysis Date = 05/12/13 Pct Recovery = 97% Analysis Date = 05/02/13 Pct Recovery = 97% Analysis Date = 05/02/13 Pct Recovery = 97% Analysis Date = 04/23/13 Pct Recovery = 97% Analysis Date = 04/23/13 Pct Recovery = 97% Analysis Date = 04/13/13 Pct Recovery = 97% Analysis Date = 04/13/13 Pct Recovery = 97% Analysis Date = 04/03/13 Pct Recovery = 97% Analysis Date = 04/03/13 Pct Recovery = 97% Analysis Date = 03/24/13 Pct Recovery = 97% Analysis Date = 03/24/13 Pct Recovery = 97% Analysis Date = 03/14/13 Pct Recovery = 97% Analysis Date = 03/14/13 Pct Recovery = 97% Analysis Date = 03/05/13 Pct Recovery = 97% Analysis Date = 03/05/13 Pct Recovery = 97% Analysis Date = 02/23/13 Pct Recovery = 97% Analysis Date = 02/23/13 Pct Recovery = 97% Analysis Date = 02/13/13 Pct Recovery = 97% Analysis Date = 02/13/13 Pct Recovery = 97% Analysis Date = 02/03/13 Pct Recovery = 97% Analysis Date = 02/03/13 Pct Recovery = 97% Analysis Date = 01/24/13 Pct Recovery = 97% Analysis Date = 01/24/13 Pct Recovery = 97% Analysis Date = 01/15/13 Pct Recovery = 97% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
EPTC

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 84 99% 13% 99% 11%
Total 84 99% 13% 99% 11%

Sample Statistics
EPTC

Characteristic N % % Basis
Plotted 84 100% Spiked
Estimated Values 2 2% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 84 .  
False Negatives 0 0% 0 out of 84
Not Spiked 50 .  
False Positives 0 0% 0 out of 50

OBSP Determination:
ETHION
METHOD: 2033 , TESTIDCODE: 82346GCM40

Laboratory ID = 20130940097 Lab Value = 0.154 Expected Conc. = 0.2595 Report level label = 0.0046 Pct Recovery = 59% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = 0507-12-04.2 Laboratory ID = 20123560092 Lab Value = 0.153 Expected Conc. = 0.2595 Report level label = 0.0046 Pct Recovery = 59% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = 0507-12-04.2 Laboratory ID = 20130810108 Lab Value = 0.202 Expected Conc. = 0.25 Report level label = 0.0046 Pct Recovery = 81% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl SpecificMix = LB92783 Laboratory ID = 20130100066 Lab Value = 0.166 Expected Conc. = 0.25 Report level label = 0.0046 Pct Recovery = 66% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl SpecificMix = LB92783 Laboratory ID = 20130510051 Lab Value = 0.070 Expected Conc. = 0.1038 Report level label = 0.0046 Pct Recovery = 68% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl SpecificMix = 0507-12-04.2 Laboratory ID = 20130390105 Lab Value = 0.070 Expected Conc. = 0.1 Report level label = 0.0046 Pct Recovery = 70% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl SpecificMix = LB92783 Laboratory ID = 20162860079 Lab Value = 0.028 Expected Conc. = 0.03 Report level label = 0.0046 Pct Recovery = 95% Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl SpecificMix = 5054800 Laboratory ID = 20161880109 Lab Value = 0.034 Expected Conc. = 0.03 Report level label = 0.0046 Pct Recovery = 113% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl SpecificMix = 5054800 Laboratory ID = 20140100085 Lab Value = 0.028 Expected Conc. = 0.03 Report level label = 0.0046 Pct Recovery = 92% Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl SpecificMix = T1130514013 Laboratory ID = 20132490342 Lab Value = 0.028 Expected Conc. = 0.03 Report level label = 0.0046 Pct Recovery = 92% Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl SpecificMix = T1130514013 Laboratory ID = 20163370001 Lab Value = 0.033 Expected Conc. = 0.0288 Report level label = 0.0046 Pct Recovery = 115% Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl SpecificMix = LC20138V Laboratory ID = 20152750006 Lab Value = 0.019 Expected Conc. = 0.028 Report level label = 0.0046 Pct Recovery = 66% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl SpecificMix = EN150514012 Laboratory ID = 20152460215 Lab Value = 0.022 Expected Conc. = 0.028 Report level label = 0.0046 Pct Recovery = 80% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl SpecificMix = EN150514012 Laboratory ID = 20171380001 Lab Value = 0.027 Expected Conc. = 0.024 Report level label = 0.0046 Pct Recovery = 114% Analysis Date = 06/07/17 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 5054800 Laboratory ID = 20170960001 Lab Value = 0.021 Expected Conc. = 0.024 Report level label = 0.0046 Pct Recovery = 89% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl SpecificMix = 5054800 Laboratory ID = 20161740258 Lab Value = 0.023 Expected Conc. = 0.024 Report level label = 0.0046 Pct Recovery = 97% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 5054800 Laboratory ID = 20171720140 Lab Value = 0.024 Expected Conc. = 0.023 Report level label = 0.0046 Pct Recovery = 102% Analysis Date = 08/31/17 SpikeMix = Supelco LC20138V: 80 µl & Phenova B20160331: 80 µl SpecificMix = LC20138V Laboratory ID = 20170740063 Lab Value = 0.025 Expected Conc. = 0.023 Report level label = 0.0046 Pct Recovery = 109% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl SpecificMix = LC20138V Laboratory ID = 20161470001 Lab Value = 0.022 Expected Conc. = 0.023 Report level label = 0.0046 Pct Recovery = 94% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl SpecificMix = LC20138V Laboratory ID = 20150720069 Lab Value = 0.022 Expected Conc. = 0.019 Report level label = 0.0046 Pct Recovery = 113% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 0227-14-08 Laboratory ID = 20141770149 Lab Value = 0.020 Expected Conc. = 0.019 Report level label = 0.0046 Pct Recovery = 108% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl SpecificMix = 0227-14-08 Laboratory ID = 20141570088 Lab Value = 0.015 Expected Conc. = 0.019 Report level label = 0.0046 Pct Recovery = 78% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl SpecificMix = 0227-14-08 Laboratory ID = 20150430092 Lab Value = 0.021 Expected Conc. = 0.0186 Report level label = 0.0046 Pct Recovery = 115% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl SpecificMix = 042814 Laboratory ID = 20143240095 Lab Value = 0.020 Expected Conc. = 0.0186 Report level label = 0.0046 Pct Recovery = 105% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl SpecificMix = 042814 Laboratory ID = 20142960086 Lab Value = 0.019 Expected Conc. = 0.0186 Report level label = 0.0046 Pct Recovery = 103% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 042814 Laboratory ID = 20142530087 Lab Value = 0.018 Expected Conc. = 0.0186 Report level label = 0.0046 Pct Recovery = 96% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl SpecificMix = 042814 Laboratory ID = 20131370001 Lab Value = 0.022 Expected Conc. = 0.0175 Report level label = 0.0046 Pct Recovery = 128% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl SpecificMix = 1473000 Laboratory ID = 20172560101 Lab Value = 0.021 Expected Conc. = 0.0155 Report level label = 0.0046 Pct Recovery = 136% Analysis Date = 12/22/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6567600: 50 µl SpecificMix = EN170808006 Laboratory ID = 20172370001 Lab Value = 0.020 Expected Conc. = 0.0155 Report level label = 0.0046 Pct Recovery = 131% Analysis Date = 11/18/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6537100: 50 µl SpecificMix = EN170808006 Laboratory ID = 20172230001 Lab Value = 0.017 Expected Conc. = 0.015 Report level label = 0.0046 Pct Recovery = 115% Analysis Date = 10/19/17 SpikeMix = ChemService 6472100: 50 µl & Abs 071717Pest: 50 µl SpecificMix = 6472100 Laboratory ID = 20140370077 Lab Value = 0.014 Expected Conc. = 0.015 Report level label = 0.0046 Pct Recovery = 91% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl SpecificMix = T1130514013 Laboratory ID = 20132690010 Lab Value = 0.015 Expected Conc. = 0.015 Report level label = 0.0046 Pct Recovery = 99% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl SpecificMix = T1130514013 Laboratory ID = 20160630046 Lab Value = 0.016 Expected Conc. = 0.014 Report level label = 0.0046 Pct Recovery = 113% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = EN150514012 Laboratory ID = 20153440001 Lab Value = 0.013 Expected Conc. = 0.014 Report level label = 0.0046 Pct Recovery = 94% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = EN150514012 Laboratory ID = 20152330039 Lab Value = 0.013 Expected Conc. = 0.014 Report level label = 0.0046 Pct Recovery = 94% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl SpecificMix = 041415 Laboratory ID = 20151900132 Lab Value = 0.013 Expected Conc. = 0.014 Report level label = 0.0046 Pct Recovery = 94% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl SpecificMix = 041415 Laboratory ID = 20151270112 Lab Value = 0.018 Expected Conc. = 0.014 Report level label = 0.0046 Pct Recovery = 128% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl SpecificMix = 041415 Laboratory ID = 20171940002 Lab Value = 0.015 Expected Conc. = 0.012 Report level label = 0.0046 Pct Recovery = 122% Analysis Date = 11/10/17 SpikeMix = ChemService 5054800: 40 µl & NSI 041816: 40 µl SpecificMix = 5054800 Laboratory ID = 20170460061 Lab Value = 0.012 Expected Conc. = 0.012 Report level label = 0.0046 Pct Recovery = 97% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl SpecificMix = 5054800 Laboratory ID = 20163560019 Lab Value = 0.016 Expected Conc. = 0.012 Report level label = 0.0046 Pct Recovery = 136% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl SpecificMix = 5054800 Laboratory ID = 20162150213 Lab Value = 0.023 Expected Conc. = 0.012 Report level label = 0.0046 Pct Recovery = 193% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl SpecificMix = 5054800 Laboratory ID = 20171510080 Lab Value = 0.012 Expected Conc. = 0.0115 Report level label = 0.0046 Pct Recovery = 102% Analysis Date = 06/09/17 SpikeMix = Supelco LC20138V: 40 µl & Crescent 03FF076: 40 µl SpecificMix = LC20138V Laboratory ID = 20162520001 Lab Value = 0.014 Expected Conc. = 0.0115 Report level label = 0.0046 Pct Recovery = 122% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl SpecificMix = LC20138V Laboratory ID = 20162660005 Lab Value = 0.012 Expected Conc. = 0.0115 Report level label = 0.0046 Pct Recovery = 102% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl SpecificMix = LC20138V Laboratory ID = 20162020124 Lab Value = 0.013 Expected Conc. = 0.0115 Report level label = 0.0046 Pct Recovery = 110% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl SpecificMix = LC20138V Laboratory ID = 20141840097 Lab Value = 0.011 Expected Conc. = 0.0095 Report level label = 0.0046 Pct Recovery = 111% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20141490205 Lab Value = 0.007 Expected Conc. = 0.0095 Report level label = 0.0046 Pct Recovery = 74% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20141420140 Lab Value = 0.009 Expected Conc. = 0.0095 Report level label = 0.0046 Pct Recovery = 93% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20141360094 Lab Value = 0.009 Expected Conc. = 0.0095 Report level label = 0.0046 Pct Recovery = 91% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20143370094 Lab Value = 0.012 Expected Conc. = 0.0093 Report level label = 0.0046 Pct Recovery = 133% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl SpecificMix = 042814 Laboratory ID = 20142820151 Lab Value = 0.010 Expected Conc. = 0.0093 Report level label = 0.0046 Pct Recovery = 112% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl SpecificMix = 042814 Laboratory ID = 20142470041 Lab Value = 0.010 Expected Conc. = 0.0093 Report level label = 0.0046 Pct Recovery = 110% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl SpecificMix = 042814 Laboratory ID = 20142200164 Lab Value = 0.010 Expected Conc. = 0.0093 Report level label = 0.0046 Pct Recovery = 110% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 042814 Laboratory ID = 20173120093 Lab Value = 0.010 Expected Conc. = 0.009 Report level label = 0.0046 Pct Recovery = 114% Analysis Date = 03/10/18 SpikeMix = ChemService 6472100: 30 µl & ChemService 6537100: 30 µl SpecificMix = 6472100 Laboratory ID = 20161050143 Lab Value = 0.008 Expected Conc. = 0.007 Report level label = 0.0046 Pct Recovery = 111% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 041415 Laboratory ID = 20160560044 Lab Value = 0.009 Expected Conc. = 0.007 Report level label = 0.0046 Pct Recovery = 121% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl SpecificMix = 041415 Laboratory ID = 20160210080 Lab Value = 0.010 Expected Conc. = 0.007 Report level label = 0.0046 Pct Recovery = 141% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 041415 Laboratory ID = 20160070059 Lab Value = 0.007 Expected Conc. = 0.007 Report level label = 0.0046 Pct Recovery = 103% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = EN150514012 Laboratory ID = 20153160001 Lab Value = 0.008 Expected Conc. = 0.007 Report level label = 0.0046 Pct Recovery = 120% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = EN150514012 Laboratory ID = 20152950078 Lab Value = 0.008 Expected Conc. = 0.007 Report level label = 0.0046 Pct Recovery = 107% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 041415 Laboratory ID = 20152040177 Lab Value = 0.009 Expected Conc. = 0.007 Report level label = 0.0046 Pct Recovery = 134% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl SpecificMix = 041415 Laboratory ID = 20151760208 Lab Value = 0.007 Expected Conc. = 0.007 Report level label = 0.0046 Pct Recovery = 106% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl SpecificMix = EN150514012 Laboratory ID = 20151480170 Lab Value = 0.006 Expected Conc. = 0.007 Report level label = 0.0046 Pct Recovery = 80% Analysis Date = 06/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150514012 Laboratory ID = 20151210037 Lab Value = 0.006 Expected Conc. = 0.007 Report level label = 0.0046 Pct Recovery = 91% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 041415 Laboratory ID = 20140730138 Lab Value = 0.007 Expected Conc. = 0.007 Report level label = 0.0046 Pct Recovery = 106% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 1473000 Laboratory ID = 20133470008 Lab Value = 0.006 Expected Conc. = 0.007 Report level label = 0.0046 Pct Recovery = 89% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl SpecificMix = 1473000 Laboratory ID = 20133310030 Lab Value = 0.009 Expected Conc. = 0.007 Report level label = 0.0046 Pct Recovery = 127% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl SpecificMix = 1473000 Laboratory ID = 20131790009 Lab Value = 0.007 Expected Conc. = 0.007 Report level label = 0.0046 Pct Recovery = 104% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl SpecificMix = 1473000 Laboratory ID = 20131650073 Lab Value = 0.008 Expected Conc. = 0.007 Report level label = 0.0046 Pct Recovery = 117% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl SpecificMix = 1473000 Laboratory ID = 20133050050 Lab Value = 0.006 Expected Conc. = 0.006 Report level label = 0.0046 Pct Recovery = 103% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl SpecificMix = T1130514013 Laboratory ID = 20132280016 Lab Value = 0.007 Expected Conc. = 0.006 Report level label = 0.0046 Pct Recovery = 117% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl SpecificMix = T1130514013 Analysis Date = 03/10/18 Pct Recovery = 118% Analysis Date = 02/28/18 Pct Recovery = 118% Analysis Date = 02/28/18 Pct Recovery = 118% Analysis Date = 02/19/18 Pct Recovery = 118% Analysis Date = 02/19/18 Pct Recovery = 118% Analysis Date = 02/09/18 Pct Recovery = 118% Analysis Date = 02/09/18 Pct Recovery = 118% Analysis Date = 01/31/18 Pct Recovery = 118% Analysis Date = 01/31/18 Pct Recovery = 118% Analysis Date = 01/22/18 Pct Recovery = 118% Analysis Date = 01/22/18 Pct Recovery = 118% Analysis Date = 01/12/18 Pct Recovery = 117% Analysis Date = 01/12/18 Pct Recovery = 117% Analysis Date = 01/03/18 Pct Recovery = 117% Analysis Date = 01/03/18 Pct Recovery = 117% Analysis Date = 12/24/17 Pct Recovery = 117% Analysis Date = 12/24/17 Pct Recovery = 117% Analysis Date = 12/15/17 Pct Recovery = 117% Analysis Date = 12/15/17 Pct Recovery = 117% Analysis Date = 12/06/17 Pct Recovery = 117% Analysis Date = 12/06/17 Pct Recovery = 117% Analysis Date = 11/26/17 Pct Recovery = 117% Analysis Date = 11/26/17 Pct Recovery = 117% Analysis Date = 11/17/17 Pct Recovery = 117% Analysis Date = 11/17/17 Pct Recovery = 117% Analysis Date = 11/07/17 Pct Recovery = 117% Analysis Date = 11/07/17 Pct Recovery = 117% Analysis Date = 10/29/17 Pct Recovery = 117% Analysis Date = 10/29/17 Pct Recovery = 117% Analysis Date = 10/20/17 Pct Recovery = 116% Analysis Date = 10/20/17 Pct Recovery = 116% Analysis Date = 10/10/17 Pct Recovery = 116% Analysis Date = 10/10/17 Pct Recovery = 116% Analysis Date = 10/01/17 Pct Recovery = 116% Analysis Date = 10/01/17 Pct Recovery = 116% Analysis Date = 09/21/17 Pct Recovery = 116% Analysis Date = 09/21/17 Pct Recovery = 116% Analysis Date = 09/12/17 Pct Recovery = 116% Analysis Date = 09/12/17 Pct Recovery = 116% Analysis Date = 09/03/17 Pct Recovery = 116% Analysis Date = 09/03/17 Pct Recovery = 116% Analysis Date = 08/24/17 Pct Recovery = 116% Analysis Date = 08/24/17 Pct Recovery = 116% Analysis Date = 08/15/17 Pct Recovery = 116% Analysis Date = 08/15/17 Pct Recovery = 116% Analysis Date = 08/05/17 Pct Recovery = 115% Analysis Date = 08/05/17 Pct Recovery = 115% Analysis Date = 07/27/17 Pct Recovery = 115% Analysis Date = 07/27/17 Pct Recovery = 115% Analysis Date = 07/18/17 Pct Recovery = 115% Analysis Date = 07/18/17 Pct Recovery = 115% Analysis Date = 07/08/17 Pct Recovery = 115% Analysis Date = 07/08/17 Pct Recovery = 115% Analysis Date = 06/29/17 Pct Recovery = 115% Analysis Date = 06/29/17 Pct Recovery = 115% Analysis Date = 06/19/17 Pct Recovery = 115% Analysis Date = 06/19/17 Pct Recovery = 115% Analysis Date = 06/10/17 Pct Recovery = 115% Analysis Date = 06/10/17 Pct Recovery = 115% Analysis Date = 06/01/17 Pct Recovery = 115% Analysis Date = 06/01/17 Pct Recovery = 115% Analysis Date = 05/22/17 Pct Recovery = 115% Analysis Date = 05/22/17 Pct Recovery = 115% Analysis Date = 05/13/17 Pct Recovery = 114% Analysis Date = 05/13/17 Pct Recovery = 114% Analysis Date = 05/03/17 Pct Recovery = 114% Analysis Date = 05/03/17 Pct Recovery = 114% Analysis Date = 04/24/17 Pct Recovery = 114% Analysis Date = 04/24/17 Pct Recovery = 114% Analysis Date = 04/15/17 Pct Recovery = 114% Analysis Date = 04/15/17 Pct Recovery = 114% Analysis Date = 04/05/17 Pct Recovery = 114% Analysis Date = 04/05/17 Pct Recovery = 114% Analysis Date = 03/27/17 Pct Recovery = 114% Analysis Date = 03/27/17 Pct Recovery = 114% Analysis Date = 03/17/17 Pct Recovery = 114% Analysis Date = 03/17/17 Pct Recovery = 114% Analysis Date = 03/08/17 Pct Recovery = 114% Analysis Date = 03/08/17 Pct Recovery = 114% Analysis Date = 02/27/17 Pct Recovery = 113% Analysis Date = 02/27/17 Pct Recovery = 113% Analysis Date = 02/17/17 Pct Recovery = 113% Analysis Date = 02/17/17 Pct Recovery = 113% Analysis Date = 02/08/17 Pct Recovery = 113% Analysis Date = 02/08/17 Pct Recovery = 113% Analysis Date = 01/29/17 Pct Recovery = 113% Analysis Date = 01/29/17 Pct Recovery = 113% Analysis Date = 01/20/17 Pct Recovery = 113% Analysis Date = 01/20/17 Pct Recovery = 113% Analysis Date = 01/11/17 Pct Recovery = 113% Analysis Date = 01/11/17 Pct Recovery = 113% Analysis Date = 01/01/17 Pct Recovery = 112% Analysis Date = 01/01/17 Pct Recovery = 112% Analysis Date = 12/23/16 Pct Recovery = 112% Analysis Date = 12/23/16 Pct Recovery = 112% Analysis Date = 12/13/16 Pct Recovery = 112% Analysis Date = 12/13/16 Pct Recovery = 112% Analysis Date = 12/04/16 Pct Recovery = 112% Analysis Date = 12/04/16 Pct Recovery = 112% Analysis Date = 11/25/16 Pct Recovery = 112% Analysis Date = 11/25/16 Pct Recovery = 112% Analysis Date = 11/15/16 Pct Recovery = 112% Analysis Date = 11/15/16 Pct Recovery = 112% Analysis Date = 11/06/16 Pct Recovery = 112% Analysis Date = 11/06/16 Pct Recovery = 112% Analysis Date = 10/27/16 Pct Recovery = 111% Analysis Date = 10/27/16 Pct Recovery = 111% Analysis Date = 10/18/16 Pct Recovery = 111% Analysis Date = 10/18/16 Pct Recovery = 111% Analysis Date = 10/09/16 Pct Recovery = 111% Analysis Date = 10/09/16 Pct Recovery = 111% Analysis Date = 09/29/16 Pct Recovery = 111% Analysis Date = 09/29/16 Pct Recovery = 111% Analysis Date = 09/20/16 Pct Recovery = 111% Analysis Date = 09/20/16 Pct Recovery = 111% Analysis Date = 09/10/16 Pct Recovery = 111% Analysis Date = 09/10/16 Pct Recovery = 111% Analysis Date = 09/01/16 Pct Recovery = 111% Analysis Date = 09/01/16 Pct Recovery = 111% Analysis Date = 08/23/16 Pct Recovery = 111% Analysis Date = 08/23/16 Pct Recovery = 111% Analysis Date = 08/13/16 Pct Recovery = 110% Analysis Date = 08/13/16 Pct Recovery = 110% Analysis Date = 08/04/16 Pct Recovery = 110% Analysis Date = 08/04/16 Pct Recovery = 110% Analysis Date = 07/25/16 Pct Recovery = 110% Analysis Date = 07/25/16 Pct Recovery = 110% Analysis Date = 07/16/16 Pct Recovery = 110% Analysis Date = 07/16/16 Pct Recovery = 110% Analysis Date = 07/07/16 Pct Recovery = 110% Analysis Date = 07/07/16 Pct Recovery = 110% Analysis Date = 06/27/16 Pct Recovery = 110% Analysis Date = 06/27/16 Pct Recovery = 110% Analysis Date = 06/18/16 Pct Recovery = 110% Analysis Date = 06/18/16 Pct Recovery = 110% Analysis Date = 06/08/16 Pct Recovery = 110% Analysis Date = 06/08/16 Pct Recovery = 110% Analysis Date = 05/30/16 Pct Recovery = 110% Analysis Date = 05/30/16 Pct Recovery = 110% Analysis Date = 05/21/16 Pct Recovery = 110% Analysis Date = 05/21/16 Pct Recovery = 110% Analysis Date = 05/11/16 Pct Recovery = 110% Analysis Date = 05/11/16 Pct Recovery = 110% Analysis Date = 05/02/16 Pct Recovery = 109% Analysis Date = 05/02/16 Pct Recovery = 109% Analysis Date = 04/22/16 Pct Recovery = 109% Analysis Date = 04/22/16 Pct Recovery = 109% Analysis Date = 04/13/16 Pct Recovery = 109% Analysis Date = 04/13/16 Pct Recovery = 109% Analysis Date = 04/04/16 Pct Recovery = 109% Analysis Date = 04/04/16 Pct Recovery = 109% Analysis Date = 03/25/16 Pct Recovery = 109% Analysis Date = 03/25/16 Pct Recovery = 109% Analysis Date = 03/16/16 Pct Recovery = 109% Analysis Date = 03/16/16 Pct Recovery = 109% Analysis Date = 03/06/16 Pct Recovery = 109% Analysis Date = 03/06/16 Pct Recovery = 109% Analysis Date = 02/26/16 Pct Recovery = 109% Analysis Date = 02/26/16 Pct Recovery = 109% Analysis Date = 02/17/16 Pct Recovery = 109% Analysis Date = 02/17/16 Pct Recovery = 109% Analysis Date = 02/07/16 Pct Recovery = 109% Analysis Date = 02/07/16 Pct Recovery = 109% Analysis Date = 01/29/16 Pct Recovery = 109% Analysis Date = 01/29/16 Pct Recovery = 109% Analysis Date = 01/19/16 Pct Recovery = 109% Analysis Date = 01/19/16 Pct Recovery = 109% Analysis Date = 01/10/16 Pct Recovery = 109% Analysis Date = 01/10/16 Pct Recovery = 109% Analysis Date = 01/01/16 Pct Recovery = 108% Analysis Date = 01/01/16 Pct Recovery = 108% Analysis Date = 12/22/15 Pct Recovery = 108% Analysis Date = 12/22/15 Pct Recovery = 108% Analysis Date = 12/13/15 Pct Recovery = 108% Analysis Date = 12/13/15 Pct Recovery = 108% Analysis Date = 12/03/15 Pct Recovery = 108% Analysis Date = 12/03/15 Pct Recovery = 108% Analysis Date = 11/24/15 Pct Recovery = 108% Analysis Date = 11/24/15 Pct Recovery = 108% Analysis Date = 11/15/15 Pct Recovery = 108% Analysis Date = 11/15/15 Pct Recovery = 108% Analysis Date = 11/05/15 Pct Recovery = 108% Analysis Date = 11/05/15 Pct Recovery = 108% Analysis Date = 10/27/15 Pct Recovery = 108% Analysis Date = 10/27/15 Pct Recovery = 108% Analysis Date = 10/17/15 Pct Recovery = 107% Analysis Date = 10/17/15 Pct Recovery = 107% Analysis Date = 10/08/15 Pct Recovery = 107% Analysis Date = 10/08/15 Pct Recovery = 107% Analysis Date = 09/29/15 Pct Recovery = 107% Analysis Date = 09/29/15 Pct Recovery = 107% Analysis Date = 09/19/15 Pct Recovery = 107% Analysis Date = 09/19/15 Pct Recovery = 107% Analysis Date = 09/10/15 Pct Recovery = 107% Analysis Date = 09/10/15 Pct Recovery = 107% Analysis Date = 08/31/15 Pct Recovery = 107% Analysis Date = 08/31/15 Pct Recovery = 107% Analysis Date = 08/22/15 Pct Recovery = 107% Analysis Date = 08/22/15 Pct Recovery = 107% Analysis Date = 08/13/15 Pct Recovery = 106% Analysis Date = 08/13/15 Pct Recovery = 106% Analysis Date = 08/03/15 Pct Recovery = 106% Analysis Date = 08/03/15 Pct Recovery = 106% Analysis Date = 07/25/15 Pct Recovery = 106% Analysis Date = 07/25/15 Pct Recovery = 106% Analysis Date = 07/15/15 Pct Recovery = 106% Analysis Date = 07/15/15 Pct Recovery = 106% Analysis Date = 07/06/15 Pct Recovery = 106% Analysis Date = 07/06/15 Pct Recovery = 106% Analysis Date = 06/27/15 Pct Recovery = 106% Analysis Date = 06/27/15 Pct Recovery = 106% Analysis Date = 06/17/15 Pct Recovery = 105% Analysis Date = 06/17/15 Pct Recovery = 105% Analysis Date = 06/08/15 Pct Recovery = 105% Analysis Date = 06/08/15 Pct Recovery = 105% Analysis Date = 05/29/15 Pct Recovery = 105% Analysis Date = 05/29/15 Pct Recovery = 105% Analysis Date = 05/20/15 Pct Recovery = 105% Analysis Date = 05/20/15 Pct Recovery = 105% Analysis Date = 05/11/15 Pct Recovery = 105% Analysis Date = 05/11/15 Pct Recovery = 105% Analysis Date = 05/01/15 Pct Recovery = 105% Analysis Date = 05/01/15 Pct Recovery = 105% Analysis Date = 04/22/15 Pct Recovery = 104% Analysis Date = 04/22/15 Pct Recovery = 104% Analysis Date = 04/12/15 Pct Recovery = 104% Analysis Date = 04/12/15 Pct Recovery = 104% Analysis Date = 04/03/15 Pct Recovery = 104% Analysis Date = 04/03/15 Pct Recovery = 104% Analysis Date = 03/25/15 Pct Recovery = 104% Analysis Date = 03/25/15 Pct Recovery = 104% Analysis Date = 03/15/15 Pct Recovery = 104% Analysis Date = 03/15/15 Pct Recovery = 104% Analysis Date = 03/06/15 Pct Recovery = 104% Analysis Date = 03/06/15 Pct Recovery = 104% Analysis Date = 02/24/15 Pct Recovery = 104% Analysis Date = 02/24/15 Pct Recovery = 104% Analysis Date = 02/15/15 Pct Recovery = 103% Analysis Date = 02/15/15 Pct Recovery = 103% Analysis Date = 02/06/15 Pct Recovery = 103% Analysis Date = 02/06/15 Pct Recovery = 103% Analysis Date = 01/27/15 Pct Recovery = 103% Analysis Date = 01/27/15 Pct Recovery = 103% Analysis Date = 01/18/15 Pct Recovery = 103% Analysis Date = 01/18/15 Pct Recovery = 103% Analysis Date = 01/08/15 Pct Recovery = 103% Analysis Date = 01/08/15 Pct Recovery = 103% Analysis Date = 12/30/14 Pct Recovery = 103% Analysis Date = 12/30/14 Pct Recovery = 103% Analysis Date = 12/21/14 Pct Recovery = 103% Analysis Date = 12/21/14 Pct Recovery = 103% Analysis Date = 12/11/14 Pct Recovery = 103% Analysis Date = 12/11/14 Pct Recovery = 103% Analysis Date = 12/02/14 Pct Recovery = 103% Analysis Date = 12/02/14 Pct Recovery = 103% Analysis Date = 11/22/14 Pct Recovery = 103% Analysis Date = 11/22/14 Pct Recovery = 103% Analysis Date = 11/13/14 Pct Recovery = 103% Analysis Date = 11/13/14 Pct Recovery = 103% Analysis Date = 11/04/14 Pct Recovery = 103% Analysis Date = 11/04/14 Pct Recovery = 103% Analysis Date = 10/25/14 Pct Recovery = 103% Analysis Date = 10/25/14 Pct Recovery = 103% Analysis Date = 10/16/14 Pct Recovery = 103% Analysis Date = 10/16/14 Pct Recovery = 103% Analysis Date = 10/06/14 Pct Recovery = 103% Analysis Date = 10/06/14 Pct Recovery = 103% Analysis Date = 09/27/14 Pct Recovery = 103% Analysis Date = 09/27/14 Pct Recovery = 103% Analysis Date = 09/18/14 Pct Recovery = 103% Analysis Date = 09/18/14 Pct Recovery = 103% Analysis Date = 09/08/14 Pct Recovery = 103% Analysis Date = 09/08/14 Pct Recovery = 103% Analysis Date = 08/30/14 Pct Recovery = 103% Analysis Date = 08/30/14 Pct Recovery = 103% Analysis Date = 08/20/14 Pct Recovery = 103% Analysis Date = 08/20/14 Pct Recovery = 103% Analysis Date = 08/11/14 Pct Recovery = 103% Analysis Date = 08/11/14 Pct Recovery = 103% Analysis Date = 08/02/14 Pct Recovery = 103% Analysis Date = 08/02/14 Pct Recovery = 103% Analysis Date = 07/23/14 Pct Recovery = 102% Analysis Date = 07/23/14 Pct Recovery = 102% Analysis Date = 07/14/14 Pct Recovery = 102% Analysis Date = 07/14/14 Pct Recovery = 102% Analysis Date = 07/04/14 Pct Recovery = 102% Analysis Date = 07/04/14 Pct Recovery = 102% Analysis Date = 06/25/14 Pct Recovery = 102% Analysis Date = 06/25/14 Pct Recovery = 102% Analysis Date = 06/16/14 Pct Recovery = 102% Analysis Date = 06/16/14 Pct Recovery = 102% Analysis Date = 06/06/14 Pct Recovery = 101% Analysis Date = 06/06/14 Pct Recovery = 101% Analysis Date = 05/28/14 Pct Recovery = 101% Analysis Date = 05/28/14 Pct Recovery = 101% Analysis Date = 05/18/14 Pct Recovery = 101% Analysis Date = 05/18/14 Pct Recovery = 101% Analysis Date = 05/09/14 Pct Recovery = 101% Analysis Date = 05/09/14 Pct Recovery = 101% Analysis Date = 04/30/14 Pct Recovery = 100% Analysis Date = 04/30/14 Pct Recovery = 100% Analysis Date = 04/20/14 Pct Recovery = 100% Analysis Date = 04/20/14 Pct Recovery = 100% Analysis Date = 04/11/14 Pct Recovery = 100% Analysis Date = 04/11/14 Pct Recovery = 100% Analysis Date = 04/01/14 Pct Recovery = 100% Analysis Date = 04/01/14 Pct Recovery = 100% Analysis Date = 03/23/14 Pct Recovery = 99% Analysis Date = 03/23/14 Pct Recovery = 99% Analysis Date = 03/14/14 Pct Recovery = 99% Analysis Date = 03/14/14 Pct Recovery = 99% Analysis Date = 03/04/14 Pct Recovery = 98% Analysis Date = 03/04/14 Pct Recovery = 98% Analysis Date = 02/23/14 Pct Recovery = 98% Analysis Date = 02/23/14 Pct Recovery = 98% Analysis Date = 02/13/14 Pct Recovery = 98% Analysis Date = 02/13/14 Pct Recovery = 98% Analysis Date = 02/04/14 Pct Recovery = 97% Analysis Date = 02/04/14 Pct Recovery = 97% Analysis Date = 01/26/14 Pct Recovery = 97% Analysis Date = 01/26/14 Pct Recovery = 97% Analysis Date = 01/16/14 Pct Recovery = 97% Analysis Date = 01/16/14 Pct Recovery = 97% Analysis Date = 01/07/14 Pct Recovery = 96% Analysis Date = 01/07/14 Pct Recovery = 96% Analysis Date = 12/28/13 Pct Recovery = 96% Analysis Date = 12/28/13 Pct Recovery = 96% Analysis Date = 12/19/13 Pct Recovery = 95% Analysis Date = 12/19/13 Pct Recovery = 95% Analysis Date = 12/10/13 Pct Recovery = 95% Analysis Date = 12/10/13 Pct Recovery = 95% Analysis Date = 11/30/13 Pct Recovery = 95% Analysis Date = 11/30/13 Pct Recovery = 95% Analysis Date = 11/21/13 Pct Recovery = 94% Analysis Date = 11/21/13 Pct Recovery = 94% Analysis Date = 11/11/13 Pct Recovery = 94% Analysis Date = 11/11/13 Pct Recovery = 94% Analysis Date = 11/02/13 Pct Recovery = 94% Analysis Date = 11/02/13 Pct Recovery = 94% Analysis Date = 10/24/13 Pct Recovery = 93% Analysis Date = 10/24/13 Pct Recovery = 93% Analysis Date = 10/14/13 Pct Recovery = 93% Analysis Date = 10/14/13 Pct Recovery = 93% Analysis Date = 10/05/13 Pct Recovery = 93% Analysis Date = 10/05/13 Pct Recovery = 93% Analysis Date = 09/25/13 Pct Recovery = 92% Analysis Date = 09/25/13 Pct Recovery = 92% Analysis Date = 09/16/13 Pct Recovery = 92% Analysis Date = 09/16/13 Pct Recovery = 92% Analysis Date = 09/07/13 Pct Recovery = 91% Analysis Date = 09/07/13 Pct Recovery = 91% Analysis Date = 08/28/13 Pct Recovery = 91% Analysis Date = 08/28/13 Pct Recovery = 91% Analysis Date = 08/19/13 Pct Recovery = 91% Analysis Date = 08/19/13 Pct Recovery = 91% Analysis Date = 08/09/13 Pct Recovery = 90% Analysis Date = 08/09/13 Pct Recovery = 90% Analysis Date = 07/31/13 Pct Recovery = 90% Analysis Date = 07/31/13 Pct Recovery = 90% Analysis Date = 07/22/13 Pct Recovery = 90% Analysis Date = 07/22/13 Pct Recovery = 90% Analysis Date = 07/12/13 Pct Recovery = 89% Analysis Date = 07/12/13 Pct Recovery = 89% Analysis Date = 07/03/13 Pct Recovery = 89% Analysis Date = 07/03/13 Pct Recovery = 89% Analysis Date = 06/23/13 Pct Recovery = 88% Analysis Date = 06/23/13 Pct Recovery = 88% Analysis Date = 06/14/13 Pct Recovery = 88% Analysis Date = 06/14/13 Pct Recovery = 88% Analysis Date = 06/05/13 Pct Recovery = 88% Analysis Date = 06/05/13 Pct Recovery = 88% Analysis Date = 05/26/13 Pct Recovery = 87% Analysis Date = 05/26/13 Pct Recovery = 87% Analysis Date = 05/17/13 Pct Recovery = 87% Analysis Date = 05/17/13 Pct Recovery = 87% Analysis Date = 05/07/13 Pct Recovery = 87% Analysis Date = 05/07/13 Pct Recovery = 87% Analysis Date = 04/28/13 Pct Recovery = 86% Analysis Date = 04/28/13 Pct Recovery = 86% Analysis Date = 04/19/13 Pct Recovery = 86% Analysis Date = 04/19/13 Pct Recovery = 86% Analysis Date = 04/09/13 Pct Recovery = 86% Analysis Date = 04/09/13 Pct Recovery = 86% Analysis Date = 03/31/13 Pct Recovery = 85% Analysis Date = 03/31/13 Pct Recovery = 85% Analysis Date = 03/21/13 Pct Recovery = 85% Analysis Date = 03/21/13 Pct Recovery = 85% Analysis Date = 03/12/13 Pct Recovery = 84% Analysis Date = 03/12/13 Pct Recovery = 84% Analysis Date = 03/03/13 Pct Recovery = 84% Analysis Date = 03/03/13 Pct Recovery = 84% Analysis Date = 02/21/13 Pct Recovery = 84% Analysis Date = 02/21/13 Pct Recovery = 84% Analysis Date = 02/12/13 Pct Recovery = 83% Analysis Date = 02/12/13 Pct Recovery = 83% Analysis Date = 02/02/13 Pct Recovery = 83% Analysis Date = 02/02/13 Pct Recovery = 83% Analysis Date = 01/24/13 Pct Recovery = 82% Analysis Date = 01/24/13 Pct Recovery = 82% Analysis Date = 01/15/13 Pct Recovery = 82% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
ETHION

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 71 104% 22% 105% 17%
Total 71 104% 22% 105% 17%

Sample Statistics
ETHION

Characteristic N % % Basis
Plotted 71 100% Spiked
Estimated Values 2 3% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 71 .  
False Negatives 0 0% 0 out of 71
Not Spiked 47 .  
False Positives 0 0% 0 out of 47

OBSP Determination:
ETHION MONOXON
METHOD: 2033 , TESTIDCODE: 61644GCM39

The SGPlot Procedure

Sample Statistics
ETHION MONOXON

Characteristic N % % Basis
Plotted 0 . Spiked
Estimated Values 0 . Spiked
Deleted Values 15 11% Spiked + Not Spiked
Spiked, Censored 0 . Spiked
Spiked 0 .  
False Negatives 0 . 0 out of 0
Not Spiked 134 .  
False Positives 1 1% 1 out of 119

OBSP Determination:
ETHOPROPHOS
METHOD: 2033 , TESTIDCODE: 82672GCM35

Laboratory ID = 20132490342 Lab Value = 0.160 Expected Conc. = 0.2 Report level label = 0.016 Pct Recovery = 80% Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20172510330 Lab Value = 0.089 Expected Conc. = 0.107 Report level label = 0.016 Pct Recovery = 83% Analysis Date = 12/29/17 SpikeMix = ChemService 6537100: 100 µl & Abs 071817Pest: 100 µl SpecificMix = 6537100 Laboratory ID = 20130810108 Lab Value = 0.082 Expected Conc. = 0.1004 Report level label = 0.016 Pct Recovery = 82% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl SpecificMix = LB92783 Laboratory ID = 20130100066 Lab Value = 0.092 Expected Conc. = 0.1004 Report level label = 0.016 Pct Recovery = 92% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl SpecificMix = LB92783 Laboratory ID = 20162860079 Lab Value = 0.098 Expected Conc. = 0.1 Report level label = 0.016 Pct Recovery = 98% Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl SpecificMix = 060916 Laboratory ID = 20163150006 Lab Value = 0.092 Expected Conc. = 0.1 Report level label = 0.016 Pct Recovery = 92% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl SpecificMix = 060916 Laboratory ID = 20140370077 Lab Value = 0.069 Expected Conc. = 0.1 Report level label = 0.016 Pct Recovery = 69% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20132560001 Lab Value = 0.097 Expected Conc. = 0.1 Report level label = 0.016 Pct Recovery = 97% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20132140002 Lab Value = 0.084 Expected Conc. = 0.1 Report level label = 0.016 Pct Recovery = 84% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl SpecificMix = LB99392 Laboratory ID = 20131370001 Lab Value = 0.113 Expected Conc. = 0.1 Report level label = 0.016 Pct Recovery = 113% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl SpecificMix = LB99392 Laboratory ID = 20130940097 Lab Value = 0.074 Expected Conc. = 0.1 Report level label = 0.016 Pct Recovery = 74% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = 0507-12-04.2 Laboratory ID = 20123560092 Lab Value = 0.073 Expected Conc. = 0.1 Report level label = 0.016 Pct Recovery = 72% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = 0507-12-04.2 Laboratory ID = 20152750006 Lab Value = 0.068 Expected Conc. = 0.096 Report level label = 0.016 Pct Recovery = 71% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl SpecificMix = 040615 Laboratory ID = 20171380001 Lab Value = 0.051 Expected Conc. = 0.0808 Report level label = 0.016 Pct Recovery = 64% Analysis Date = 06/07/17 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 041816 Laboratory ID = 20170740063 Lab Value = 0.071 Expected Conc. = 0.0808 Report level label = 0.016 Pct Recovery = 88% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl SpecificMix = 041816 Laboratory ID = 20161740258 Lab Value = 0.045 Expected Conc. = 0.0808 Report level label = 0.016 Pct Recovery = 56% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 041816 Laboratory ID = 20171660002 Lab Value = 0.077 Expected Conc. = 0.08 Report level label = 0.016 Pct Recovery = 96% Analysis Date = 08/23/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = 060916 Laboratory ID = 20170190026 Lab Value = 0.074 Expected Conc. = 0.08 Report level label = 0.016 Pct Recovery = 92% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = 060916 Laboratory ID = 20150430092 Lab Value = 0.056 Expected Conc. = 0.066 Report level label = 0.016 Pct Recovery = 84% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl SpecificMix = E1140407002 Laboratory ID = 20143110108 Lab Value = 0.054 Expected Conc. = 0.066 Report level label = 0.016 Pct Recovery = 82% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl SpecificMix = E1140407002 Laboratory ID = 20142720002 Lab Value = 0.050 Expected Conc. = 0.066 Report level label = 0.016 Pct Recovery = 76% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl SpecificMix = E1140407002 Laboratory ID = 20141770149 Lab Value = 0.053 Expected Conc. = 0.066 Report level label = 0.016 Pct Recovery = 80% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl SpecificMix = E1140407002 Laboratory ID = 20143240095 Lab Value = 0.066 Expected Conc. = 0.0642 Report level label = 0.016 Pct Recovery = 103% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl SpecificMix = 032714 Laboratory ID = 20142270001 Lab Value = 0.045 Expected Conc. = 0.0642 Report level label = 0.016 Pct Recovery = 70% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl SpecificMix = 032714 Laboratory ID = 20141220025 Lab Value = 0.064 Expected Conc. = 0.0642 Report level label = 0.016 Pct Recovery = 100% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl SpecificMix = 032714 Laboratory ID = 20172370001 Lab Value = 0.047 Expected Conc. = 0.0535 Report level label = 0.016 Pct Recovery = 88% Analysis Date = 11/18/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6537100: 50 µl SpecificMix = 6537100 Laboratory ID = 20172230001 Lab Value = 0.070 Expected Conc. = 0.0535 Report level label = 0.016 Pct Recovery = 130% Analysis Date = 10/19/17 SpikeMix = ChemService 6472100: 50 µl & Abs 071717Pest: 50 µl SpecificMix = 071717Pest Laboratory ID = 20161260151 Lab Value = 0.041 Expected Conc. = 0.048 Report level label = 0.016 Pct Recovery = 85% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = EN150513008 Laboratory ID = 20160770090 Lab Value = 0.041 Expected Conc. = 0.048 Report level label = 0.016 Pct Recovery = 86% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = EN150513008 Laboratory ID = 20153510109 Lab Value = 0.033 Expected Conc. = 0.048 Report level label = 0.016 Pct Recovery = 69% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = EN150513008 Laboratory ID = 20152330039 Lab Value = 0.038 Expected Conc. = 0.048 Report level label = 0.016 Pct Recovery = 79% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl SpecificMix = EN150513008 Laboratory ID = 20151550293 Lab Value = 0.050 Expected Conc. = 0.048 Report level label = 0.016 Pct Recovery = 104% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl SpecificMix = 040615 Laboratory ID = 20172020035 Lab Value = 0.056 Expected Conc. = 0.0428 Report level label = 0.016 Pct Recovery = 130% Analysis Date = 11/07/17 SpikeMix = Abs 071717Pest: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 071717Pest Laboratory ID = 20171940002 Lab Value = 0.038 Expected Conc. = 0.0404 Report level label = 0.016 Pct Recovery = 95% Analysis Date = 11/10/17 SpikeMix = ChemService 5054800: 40 µl & NSI 041816: 40 µl SpecificMix = 041816 Laboratory ID = 20161600087 Lab Value = 0.035 Expected Conc. = 0.0404 Report level label = 0.016 Pct Recovery = 86% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 041816 Laboratory ID = 20161340228 Lab Value = 0.029 Expected Conc. = 0.0404 Report level label = 0.016 Pct Recovery = 73% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl SpecificMix = 041816 Laboratory ID = 20130390105 Lab Value = 0.029 Expected Conc. = 0.0402 Report level label = 0.016 Pct Recovery = 73% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl SpecificMix = LB92783 Laboratory ID = 20171160110 Lab Value = 0.037 Expected Conc. = 0.04 Report level label = 0.016 Pct Recovery = 91% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = 060916 Laboratory ID = 20162520001 Lab Value = 0.056 Expected Conc. = 0.04 Report level label = 0.016 Pct Recovery = 139% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl SpecificMix = 060916 Laboratory ID = 20163560019 Lab Value = 0.038 Expected Conc. = 0.04 Report level label = 0.016 Pct Recovery = 95% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl SpecificMix = 060916 Laboratory ID = 20162380004 Lab Value = 0.043 Expected Conc. = 0.04 Report level label = 0.016 Pct Recovery = 107% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = 060916 Laboratory ID = 20140510043 Lab Value = 0.043 Expected Conc. = 0.04 Report level label = 0.016 Pct Recovery = 107% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl SpecificMix = LB99392 Laboratory ID = 20133580036 Lab Value = 0.024 Expected Conc. = 0.04 Report level label = 0.016 Pct Recovery = 61% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20133470008 Lab Value = 0.034 Expected Conc. = 0.04 Report level label = 0.016 Pct Recovery = 84% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl SpecificMix = LB99392 Laboratory ID = 20133190012 Lab Value = 0.043 Expected Conc. = 0.04 Report level label = 0.016 Pct Recovery = 107% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = LB99392 Laboratory ID = 20133050050 Lab Value = 0.046 Expected Conc. = 0.04 Report level label = 0.016 Pct Recovery = 115% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl SpecificMix = LB99392 Laboratory ID = 20131790009 Lab Value = 0.029 Expected Conc. = 0.04 Report level label = 0.016 Pct Recovery = 72% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20131510026 Lab Value = 0.037 Expected Conc. = 0.04 Report level label = 0.016 Pct Recovery = 94% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20130510051 Lab Value = 0.030 Expected Conc. = 0.04 Report level label = 0.016 Pct Recovery = 75% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl SpecificMix = 0507-12-04.2 Laboratory ID = 20142470041 Lab Value = 0.034 Expected Conc. = 0.033 Report level label = 0.016 Pct Recovery = 103% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141910243 Lab Value = 0.026 Expected Conc. = 0.033 Report level label = 0.016 Pct Recovery = 78% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141640076 Lab Value = 0.031 Expected Conc. = 0.033 Report level label = 0.016 Pct Recovery = 93% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141360094 Lab Value = 0.027 Expected Conc. = 0.033 Report level label = 0.016 Pct Recovery = 81% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = E1140407002 Laboratory ID = 20173120093 Lab Value = 0.039 Expected Conc. = 0.0321 Report level label = 0.016 Pct Recovery = 122% Analysis Date = 03/10/18 SpikeMix = ChemService 6472100: 30 µl & ChemService 6537100: 30 µl SpecificMix = 6537100 Laboratory ID = 20172780018 Lab Value = 0.027 Expected Conc. = 0.0321 Report level label = 0.016 Pct Recovery = 83% Analysis Date = 02/08/18 SpikeMix = ChemService 6537100: 30 µl & Abs 071817Pest: 30 µl SpecificMix = 6537100 Laboratory ID = 20150150115 Lab Value = 0.025 Expected Conc. = 0.0321 Report level label = 0.016 Pct Recovery = 77% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl SpecificMix = 032714 Laboratory ID = 20142820151 Lab Value = 0.032 Expected Conc. = 0.0321 Report level label = 0.016 Pct Recovery = 100% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl SpecificMix = 032714 Laboratory ID = 20141490205 Lab Value = 0.039 Expected Conc. = 0.0321 Report level label = 0.016 Pct Recovery = 120% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = 032714 Laboratory ID = 20141080004 Lab Value = 0.029 Expected Conc. = 0.0321 Report level label = 0.016 Pct Recovery = 92% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl SpecificMix = 032714 Laboratory ID = 20160070059 Lab Value = 0.019 Expected Conc. = 0.024 Report level label = 0.016 Pct Recovery = 79% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = 040615 Laboratory ID = 20153160001 Lab Value = 0.021 Expected Conc. = 0.024 Report level label = 0.016 Pct Recovery = 86% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = EN150513008 Laboratory ID = 20153030068 Lab Value = 0.022 Expected Conc. = 0.024 Report level label = 0.016 Pct Recovery = 93% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150513008 Laboratory ID = 20152190003 Lab Value = 0.019 Expected Conc. = 0.024 Report level label = 0.016 Pct Recovery = 77% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150513008 Laboratory ID = 20151480170 Lab Value = 0.022 Expected Conc. = 0.024 Report level label = 0.016 Pct Recovery = 93% Analysis Date = 06/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150513008 Laboratory ID = 20151380009 Lab Value = 0.026 Expected Conc. = 0.024 Report level label = 0.016 Pct Recovery = 107% Analysis Date = 05/30/15 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Laboratory ID = 20151210037 Lab Value = 0.026 Expected Conc. = 0.024 Report level label = 0.016 Pct Recovery = 109% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Analysis Date = 03/10/18 Pct Recovery = 105% Analysis Date = 02/28/18 Pct Recovery = 104% Analysis Date = 02/28/18 Pct Recovery = 104% Analysis Date = 02/19/18 Pct Recovery = 104% Analysis Date = 02/19/18 Pct Recovery = 104% Analysis Date = 02/09/18 Pct Recovery = 104% Analysis Date = 02/09/18 Pct Recovery = 104% Analysis Date = 01/31/18 Pct Recovery = 103% Analysis Date = 01/31/18 Pct Recovery = 103% Analysis Date = 01/22/18 Pct Recovery = 103% Analysis Date = 01/22/18 Pct Recovery = 103% Analysis Date = 01/12/18 Pct Recovery = 103% Analysis Date = 01/12/18 Pct Recovery = 103% Analysis Date = 01/03/18 Pct Recovery = 103% Analysis Date = 01/03/18 Pct Recovery = 103% Analysis Date = 12/24/17 Pct Recovery = 102% Analysis Date = 12/24/17 Pct Recovery = 102% Analysis Date = 12/15/17 Pct Recovery = 102% Analysis Date = 12/15/17 Pct Recovery = 102% Analysis Date = 12/06/17 Pct Recovery = 102% Analysis Date = 12/06/17 Pct Recovery = 102% Analysis Date = 11/26/17 Pct Recovery = 101% Analysis Date = 11/26/17 Pct Recovery = 101% Analysis Date = 11/17/17 Pct Recovery = 101% Analysis Date = 11/17/17 Pct Recovery = 101% Analysis Date = 11/07/17 Pct Recovery = 101% Analysis Date = 11/07/17 Pct Recovery = 101% Analysis Date = 10/29/17 Pct Recovery = 101% Analysis Date = 10/29/17 Pct Recovery = 101% Analysis Date = 10/20/17 Pct Recovery = 100% Analysis Date = 10/20/17 Pct Recovery = 100% Analysis Date = 10/10/17 Pct Recovery = 100% Analysis Date = 10/10/17 Pct Recovery = 100% Analysis Date = 10/01/17 Pct Recovery = 100% Analysis Date = 10/01/17 Pct Recovery = 100% Analysis Date = 09/21/17 Pct Recovery = 100% Analysis Date = 09/21/17 Pct Recovery = 100% Analysis Date = 09/12/17 Pct Recovery = 99% Analysis Date = 09/12/17 Pct Recovery = 99% Analysis Date = 09/03/17 Pct Recovery = 99% Analysis Date = 09/03/17 Pct Recovery = 99% Analysis Date = 08/24/17 Pct Recovery = 99% Analysis Date = 08/24/17 Pct Recovery = 99% Analysis Date = 08/15/17 Pct Recovery = 98% Analysis Date = 08/15/17 Pct Recovery = 98% Analysis Date = 08/05/17 Pct Recovery = 98% Analysis Date = 08/05/17 Pct Recovery = 98% Analysis Date = 07/27/17 Pct Recovery = 98% Analysis Date = 07/27/17 Pct Recovery = 98% Analysis Date = 07/18/17 Pct Recovery = 98% Analysis Date = 07/18/17 Pct Recovery = 98% Analysis Date = 07/08/17 Pct Recovery = 97% Analysis Date = 07/08/17 Pct Recovery = 97% Analysis Date = 06/29/17 Pct Recovery = 97% Analysis Date = 06/29/17 Pct Recovery = 97% Analysis Date = 06/19/17 Pct Recovery = 97% Analysis Date = 06/19/17 Pct Recovery = 97% Analysis Date = 06/10/17 Pct Recovery = 97% Analysis Date = 06/10/17 Pct Recovery = 97% Analysis Date = 06/01/17 Pct Recovery = 96% Analysis Date = 06/01/17 Pct Recovery = 96% Analysis Date = 05/22/17 Pct Recovery = 96% Analysis Date = 05/22/17 Pct Recovery = 96% Analysis Date = 05/13/17 Pct Recovery = 96% Analysis Date = 05/13/17 Pct Recovery = 96% Analysis Date = 05/03/17 Pct Recovery = 96% Analysis Date = 05/03/17 Pct Recovery = 96% Analysis Date = 04/24/17 Pct Recovery = 95% Analysis Date = 04/24/17 Pct Recovery = 95% Analysis Date = 04/15/17 Pct Recovery = 95% Analysis Date = 04/15/17 Pct Recovery = 95% Analysis Date = 04/05/17 Pct Recovery = 95% Analysis Date = 04/05/17 Pct Recovery = 95% Analysis Date = 03/27/17 Pct Recovery = 95% Analysis Date = 03/27/17 Pct Recovery = 95% Analysis Date = 03/17/17 Pct Recovery = 94% Analysis Date = 03/17/17 Pct Recovery = 94% Analysis Date = 03/08/17 Pct Recovery = 94% Analysis Date = 03/08/17 Pct Recovery = 94% Analysis Date = 02/27/17 Pct Recovery = 94% Analysis Date = 02/27/17 Pct Recovery = 94% Analysis Date = 02/17/17 Pct Recovery = 94% Analysis Date = 02/17/17 Pct Recovery = 94% Analysis Date = 02/08/17 Pct Recovery = 93% Analysis Date = 02/08/17 Pct Recovery = 93% Analysis Date = 01/29/17 Pct Recovery = 93% Analysis Date = 01/29/17 Pct Recovery = 93% Analysis Date = 01/20/17 Pct Recovery = 93% Analysis Date = 01/20/17 Pct Recovery = 93% Analysis Date = 01/11/17 Pct Recovery = 93% Analysis Date = 01/11/17 Pct Recovery = 93% Analysis Date = 01/01/17 Pct Recovery = 92% Analysis Date = 01/01/17 Pct Recovery = 92% Analysis Date = 12/23/16 Pct Recovery = 92% Analysis Date = 12/23/16 Pct Recovery = 92% Analysis Date = 12/13/16 Pct Recovery = 92% Analysis Date = 12/13/16 Pct Recovery = 92% Analysis Date = 12/04/16 Pct Recovery = 92% Analysis Date = 12/04/16 Pct Recovery = 92% Analysis Date = 11/25/16 Pct Recovery = 91% Analysis Date = 11/25/16 Pct Recovery = 91% Analysis Date = 11/15/16 Pct Recovery = 91% Analysis Date = 11/15/16 Pct Recovery = 91% Analysis Date = 11/06/16 Pct Recovery = 91% Analysis Date = 11/06/16 Pct Recovery = 91% Analysis Date = 10/27/16 Pct Recovery = 91% Analysis Date = 10/27/16 Pct Recovery = 91% Analysis Date = 10/18/16 Pct Recovery = 91% Analysis Date = 10/18/16 Pct Recovery = 91% Analysis Date = 10/09/16 Pct Recovery = 91% Analysis Date = 10/09/16 Pct Recovery = 91% Analysis Date = 09/29/16 Pct Recovery = 90% Analysis Date = 09/29/16 Pct Recovery = 90% Analysis Date = 09/20/16 Pct Recovery = 90% Analysis Date = 09/20/16 Pct Recovery = 90% Analysis Date = 09/10/16 Pct Recovery = 90% Analysis Date = 09/10/16 Pct Recovery = 90% Analysis Date = 09/01/16 Pct Recovery = 90% Analysis Date = 09/01/16 Pct Recovery = 90% Analysis Date = 08/23/16 Pct Recovery = 90% Analysis Date = 08/23/16 Pct Recovery = 90% Analysis Date = 08/13/16 Pct Recovery = 89% Analysis Date = 08/13/16 Pct Recovery = 89% Analysis Date = 08/04/16 Pct Recovery = 89% Analysis Date = 08/04/16 Pct Recovery = 89% Analysis Date = 07/25/16 Pct Recovery = 89% Analysis Date = 07/25/16 Pct Recovery = 89% Analysis Date = 07/16/16 Pct Recovery = 89% Analysis Date = 07/16/16 Pct Recovery = 89% Analysis Date = 07/07/16 Pct Recovery = 89% Analysis Date = 07/07/16 Pct Recovery = 89% Analysis Date = 06/27/16 Pct Recovery = 88% Analysis Date = 06/27/16 Pct Recovery = 88% Analysis Date = 06/18/16 Pct Recovery = 88% Analysis Date = 06/18/16 Pct Recovery = 88% Analysis Date = 06/08/16 Pct Recovery = 88% Analysis Date = 06/08/16 Pct Recovery = 88% Analysis Date = 05/30/16 Pct Recovery = 88% Analysis Date = 05/30/16 Pct Recovery = 88% Analysis Date = 05/21/16 Pct Recovery = 88% Analysis Date = 05/21/16 Pct Recovery = 88% Analysis Date = 05/11/16 Pct Recovery = 87% Analysis Date = 05/11/16 Pct Recovery = 87% Analysis Date = 05/02/16 Pct Recovery = 87% Analysis Date = 05/02/16 Pct Recovery = 87% Analysis Date = 04/22/16 Pct Recovery = 87% Analysis Date = 04/22/16 Pct Recovery = 87% Analysis Date = 04/13/16 Pct Recovery = 87% Analysis Date = 04/13/16 Pct Recovery = 87% Analysis Date = 04/04/16 Pct Recovery = 87% Analysis Date = 04/04/16 Pct Recovery = 87% Analysis Date = 03/25/16 Pct Recovery = 87% Analysis Date = 03/25/16 Pct Recovery = 87% Analysis Date = 03/16/16 Pct Recovery = 87% Analysis Date = 03/16/16 Pct Recovery = 87% Analysis Date = 03/06/16 Pct Recovery = 87% Analysis Date = 03/06/16 Pct Recovery = 87% Analysis Date = 02/26/16 Pct Recovery = 87% Analysis Date = 02/26/16 Pct Recovery = 87% Analysis Date = 02/17/16 Pct Recovery = 87% Analysis Date = 02/17/16 Pct Recovery = 87% Analysis Date = 02/07/16 Pct Recovery = 87% Analysis Date = 02/07/16 Pct Recovery = 87% Analysis Date = 01/29/16 Pct Recovery = 87% Analysis Date = 01/29/16 Pct Recovery = 87% Analysis Date = 01/19/16 Pct Recovery = 87% Analysis Date = 01/19/16 Pct Recovery = 87% Analysis Date = 01/10/16 Pct Recovery = 87% Analysis Date = 01/10/16 Pct Recovery = 87% Analysis Date = 01/01/16 Pct Recovery = 87% Analysis Date = 01/01/16 Pct Recovery = 87% Analysis Date = 12/22/15 Pct Recovery = 87% Analysis Date = 12/22/15 Pct Recovery = 87% Analysis Date = 12/13/15 Pct Recovery = 87% Analysis Date = 12/13/15 Pct Recovery = 87% Analysis Date = 12/03/15 Pct Recovery = 87% Analysis Date = 12/03/15 Pct Recovery = 87% Analysis Date = 11/24/15 Pct Recovery = 87% Analysis Date = 11/24/15 Pct Recovery = 87% Analysis Date = 11/15/15 Pct Recovery = 86% Analysis Date = 11/15/15 Pct Recovery = 86% Analysis Date = 11/05/15 Pct Recovery = 86% Analysis Date = 11/05/15 Pct Recovery = 86% Analysis Date = 10/27/15 Pct Recovery = 86% Analysis Date = 10/27/15 Pct Recovery = 86% Analysis Date = 10/17/15 Pct Recovery = 86% Analysis Date = 10/17/15 Pct Recovery = 86% Analysis Date = 10/08/15 Pct Recovery = 86% Analysis Date = 10/08/15 Pct Recovery = 86% Analysis Date = 09/29/15 Pct Recovery = 86% Analysis Date = 09/29/15 Pct Recovery = 86% Analysis Date = 09/19/15 Pct Recovery = 86% Analysis Date = 09/19/15 Pct Recovery = 86% Analysis Date = 09/10/15 Pct Recovery = 86% Analysis Date = 09/10/15 Pct Recovery = 86% Analysis Date = 08/31/15 Pct Recovery = 86% Analysis Date = 08/31/15 Pct Recovery = 86% Analysis Date = 08/22/15 Pct Recovery = 86% Analysis Date = 08/22/15 Pct Recovery = 86% Analysis Date = 08/13/15 Pct Recovery = 86% Analysis Date = 08/13/15 Pct Recovery = 86% Analysis Date = 08/03/15 Pct Recovery = 86% Analysis Date = 08/03/15 Pct Recovery = 86% Analysis Date = 07/25/15 Pct Recovery = 87% Analysis Date = 07/25/15 Pct Recovery = 87% Analysis Date = 07/15/15 Pct Recovery = 87% Analysis Date = 07/15/15 Pct Recovery = 87% Analysis Date = 07/06/15 Pct Recovery = 87% Analysis Date = 07/06/15 Pct Recovery = 87% Analysis Date = 06/27/15 Pct Recovery = 87% Analysis Date = 06/27/15 Pct Recovery = 87% Analysis Date = 06/17/15 Pct Recovery = 87% Analysis Date = 06/17/15 Pct Recovery = 87% Analysis Date = 06/08/15 Pct Recovery = 87% Analysis Date = 06/08/15 Pct Recovery = 87% Analysis Date = 05/29/15 Pct Recovery = 87% Analysis Date = 05/29/15 Pct Recovery = 87% Analysis Date = 05/20/15 Pct Recovery = 88% Analysis Date = 05/20/15 Pct Recovery = 88% Analysis Date = 05/11/15 Pct Recovery = 88% Analysis Date = 05/11/15 Pct Recovery = 88% Analysis Date = 05/01/15 Pct Recovery = 88% Analysis Date = 05/01/15 Pct Recovery = 88% Analysis Date = 04/22/15 Pct Recovery = 88% Analysis Date = 04/22/15 Pct Recovery = 88% Analysis Date = 04/12/15 Pct Recovery = 88% Analysis Date = 04/12/15 Pct Recovery = 88% Analysis Date = 04/03/15 Pct Recovery = 88% Analysis Date = 04/03/15 Pct Recovery = 88% Analysis Date = 03/25/15 Pct Recovery = 89% Analysis Date = 03/25/15 Pct Recovery = 89% Analysis Date = 03/15/15 Pct Recovery = 89% Analysis Date = 03/15/15 Pct Recovery = 89% Analysis Date = 03/06/15 Pct Recovery = 89% Analysis Date = 03/06/15 Pct Recovery = 89% Analysis Date = 02/24/15 Pct Recovery = 89% Analysis Date = 02/24/15 Pct Recovery = 89% Analysis Date = 02/15/15 Pct Recovery = 89% Analysis Date = 02/15/15 Pct Recovery = 89% Analysis Date = 02/06/15 Pct Recovery = 89% Analysis Date = 02/06/15 Pct Recovery = 89% Analysis Date = 01/27/15 Pct Recovery = 89% Analysis Date = 01/27/15 Pct Recovery = 89% Analysis Date = 01/18/15 Pct Recovery = 89% Analysis Date = 01/18/15 Pct Recovery = 89% Analysis Date = 01/08/15 Pct Recovery = 90% Analysis Date = 01/08/15 Pct Recovery = 90% Analysis Date = 12/30/14 Pct Recovery = 90% Analysis Date = 12/30/14 Pct Recovery = 90% Analysis Date = 12/21/14 Pct Recovery = 90% Analysis Date = 12/21/14 Pct Recovery = 90% Analysis Date = 12/11/14 Pct Recovery = 90% Analysis Date = 12/11/14 Pct Recovery = 90% Analysis Date = 12/02/14 Pct Recovery = 90% Analysis Date = 12/02/14 Pct Recovery = 90% Analysis Date = 11/22/14 Pct Recovery = 90% Analysis Date = 11/22/14 Pct Recovery = 90% Analysis Date = 11/13/14 Pct Recovery = 90% Analysis Date = 11/13/14 Pct Recovery = 90% Analysis Date = 11/04/14 Pct Recovery = 90% Analysis Date = 11/04/14 Pct Recovery = 90% Analysis Date = 10/25/14 Pct Recovery = 90% Analysis Date = 10/25/14 Pct Recovery = 90% Analysis Date = 10/16/14 Pct Recovery = 90% Analysis Date = 10/16/14 Pct Recovery = 90% Analysis Date = 10/06/14 Pct Recovery = 90% Analysis Date = 10/06/14 Pct Recovery = 90% Analysis Date = 09/27/14 Pct Recovery = 90% Analysis Date = 09/27/14 Pct Recovery = 90% Analysis Date = 09/18/14 Pct Recovery = 90% Analysis Date = 09/18/14 Pct Recovery = 90% Analysis Date = 09/08/14 Pct Recovery = 90% Analysis Date = 09/08/14 Pct Recovery = 90% Analysis Date = 08/30/14 Pct Recovery = 90% Analysis Date = 08/30/14 Pct Recovery = 90% Analysis Date = 08/20/14 Pct Recovery = 90% Analysis Date = 08/20/14 Pct Recovery = 90% Analysis Date = 08/11/14 Pct Recovery = 90% Analysis Date = 08/11/14 Pct Recovery = 90% Analysis Date = 08/02/14 Pct Recovery = 90% Analysis Date = 08/02/14 Pct Recovery = 90% Analysis Date = 07/23/14 Pct Recovery = 90% Analysis Date = 07/23/14 Pct Recovery = 90% Analysis Date = 07/14/14 Pct Recovery = 90% Analysis Date = 07/14/14 Pct Recovery = 90% Analysis Date = 07/04/14 Pct Recovery = 90% Analysis Date = 07/04/14 Pct Recovery = 90% Analysis Date = 06/25/14 Pct Recovery = 90% Analysis Date = 06/25/14 Pct Recovery = 90% Analysis Date = 06/16/14 Pct Recovery = 90% Analysis Date = 06/16/14 Pct Recovery = 90% Analysis Date = 06/06/14 Pct Recovery = 90% Analysis Date = 06/06/14 Pct Recovery = 90% Analysis Date = 05/28/14 Pct Recovery = 90% Analysis Date = 05/28/14 Pct Recovery = 90% Analysis Date = 05/18/14 Pct Recovery = 90% Analysis Date = 05/18/14 Pct Recovery = 90% Analysis Date = 05/09/14 Pct Recovery = 90% Analysis Date = 05/09/14 Pct Recovery = 90% Analysis Date = 04/30/14 Pct Recovery = 89% Analysis Date = 04/30/14 Pct Recovery = 89% Analysis Date = 04/20/14 Pct Recovery = 89% Analysis Date = 04/20/14 Pct Recovery = 89% Analysis Date = 04/11/14 Pct Recovery = 89% Analysis Date = 04/11/14 Pct Recovery = 89% Analysis Date = 04/01/14 Pct Recovery = 89% Analysis Date = 04/01/14 Pct Recovery = 89% Analysis Date = 03/23/14 Pct Recovery = 89% Analysis Date = 03/23/14 Pct Recovery = 89% Analysis Date = 03/14/14 Pct Recovery = 89% Analysis Date = 03/14/14 Pct Recovery = 89% Analysis Date = 03/04/14 Pct Recovery = 89% Analysis Date = 03/04/14 Pct Recovery = 89% Analysis Date = 02/23/14 Pct Recovery = 89% Analysis Date = 02/23/14 Pct Recovery = 89% Analysis Date = 02/13/14 Pct Recovery = 89% Analysis Date = 02/13/14 Pct Recovery = 89% Analysis Date = 02/04/14 Pct Recovery = 89% Analysis Date = 02/04/14 Pct Recovery = 89% Analysis Date = 01/26/14 Pct Recovery = 88% Analysis Date = 01/26/14 Pct Recovery = 88% Analysis Date = 01/16/14 Pct Recovery = 88% Analysis Date = 01/16/14 Pct Recovery = 88% Analysis Date = 01/07/14 Pct Recovery = 88% Analysis Date = 01/07/14 Pct Recovery = 88% Analysis Date = 12/28/13 Pct Recovery = 88% Analysis Date = 12/28/13 Pct Recovery = 88% Analysis Date = 12/19/13 Pct Recovery = 88% Analysis Date = 12/19/13 Pct Recovery = 88% Analysis Date = 12/10/13 Pct Recovery = 88% Analysis Date = 12/10/13 Pct Recovery = 88% Analysis Date = 11/30/13 Pct Recovery = 88% Analysis Date = 11/30/13 Pct Recovery = 88% Analysis Date = 11/21/13 Pct Recovery = 87% Analysis Date = 11/21/13 Pct Recovery = 87% Analysis Date = 11/11/13 Pct Recovery = 87% Analysis Date = 11/11/13 Pct Recovery = 87% Analysis Date = 11/02/13 Pct Recovery = 87% Analysis Date = 11/02/13 Pct Recovery = 87% Analysis Date = 10/24/13 Pct Recovery = 87% Analysis Date = 10/24/13 Pct Recovery = 87% Analysis Date = 10/14/13 Pct Recovery = 87% Analysis Date = 10/14/13 Pct Recovery = 87% Analysis Date = 10/05/13 Pct Recovery = 87% Analysis Date = 10/05/13 Pct Recovery = 87% Analysis Date = 09/25/13 Pct Recovery = 87% Analysis Date = 09/25/13 Pct Recovery = 87% Analysis Date = 09/16/13 Pct Recovery = 86% Analysis Date = 09/16/13 Pct Recovery = 86% Analysis Date = 09/07/13 Pct Recovery = 86% Analysis Date = 09/07/13 Pct Recovery = 86% Analysis Date = 08/28/13 Pct Recovery = 86% Analysis Date = 08/28/13 Pct Recovery = 86% Analysis Date = 08/19/13 Pct Recovery = 86% Analysis Date = 08/19/13 Pct Recovery = 86% Analysis Date = 08/09/13 Pct Recovery = 86% Analysis Date = 08/09/13 Pct Recovery = 86% Analysis Date = 07/31/13 Pct Recovery = 86% Analysis Date = 07/31/13 Pct Recovery = 86% Analysis Date = 07/22/13 Pct Recovery = 86% Analysis Date = 07/22/13 Pct Recovery = 86% Analysis Date = 07/12/13 Pct Recovery = 86% Analysis Date = 07/12/13 Pct Recovery = 86% Analysis Date = 07/03/13 Pct Recovery = 85% Analysis Date = 07/03/13 Pct Recovery = 85% Analysis Date = 06/23/13 Pct Recovery = 85% Analysis Date = 06/23/13 Pct Recovery = 85% Analysis Date = 06/14/13 Pct Recovery = 85% Analysis Date = 06/14/13 Pct Recovery = 85% Analysis Date = 06/05/13 Pct Recovery = 85% Analysis Date = 06/05/13 Pct Recovery = 85% Analysis Date = 05/26/13 Pct Recovery = 85% Analysis Date = 05/26/13 Pct Recovery = 85% Analysis Date = 05/17/13 Pct Recovery = 85% Analysis Date = 05/17/13 Pct Recovery = 85% Analysis Date = 05/07/13 Pct Recovery = 85% Analysis Date = 05/07/13 Pct Recovery = 85% Analysis Date = 04/28/13 Pct Recovery = 84% Analysis Date = 04/28/13 Pct Recovery = 84% Analysis Date = 04/19/13 Pct Recovery = 84% Analysis Date = 04/19/13 Pct Recovery = 84% Analysis Date = 04/09/13 Pct Recovery = 84% Analysis Date = 04/09/13 Pct Recovery = 84% Analysis Date = 03/31/13 Pct Recovery = 84% Analysis Date = 03/31/13 Pct Recovery = 84% Analysis Date = 03/21/13 Pct Recovery = 84% Analysis Date = 03/21/13 Pct Recovery = 84% Analysis Date = 03/12/13 Pct Recovery = 84% Analysis Date = 03/12/13 Pct Recovery = 84% Analysis Date = 03/03/13 Pct Recovery = 84% Analysis Date = 03/03/13 Pct Recovery = 84% Analysis Date = 02/21/13 Pct Recovery = 83% Analysis Date = 02/21/13 Pct Recovery = 83% Analysis Date = 02/12/13 Pct Recovery = 83% Analysis Date = 02/12/13 Pct Recovery = 83% Analysis Date = 02/02/13 Pct Recovery = 83% Analysis Date = 02/02/13 Pct Recovery = 83% Analysis Date = 01/24/13 Pct Recovery = 83% Analysis Date = 01/24/13 Pct Recovery = 83% Analysis Date = 01/15/13 Pct Recovery = 83% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
ETHOPROPHOS

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 66 90% 17% 87% 16%
Total 66 90% 17% 87% 16%

Sample Statistics
ETHOPROPHOS

Characteristic N % % Basis
Plotted 66 90% Spiked
Estimated Values 7 10% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 1 1% Spiked
Spiked 73 .  
False Negatives 6 8% 6 out of 73
Not Spiked 45 .  
False Positives 0 0% 0 out of 45

OBSP Determination:
FENAMIPHOS
METHOD: 2033 , TESTIDCODE: 61591GCM39

Laboratory ID = 20130250061 Lab Value = 0.208 Expected Conc. = 0.49 Report level label = 0.03 Pct Recovery = 42% Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl SpecificMix = 05BB029 Laboratory ID = 20140100085 Lab Value = 0.226 Expected Conc. = 0.326 Report level label = 0.03 Pct Recovery = 69% Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl SpecificMix = 042413 Laboratory ID = 20140230082 Lab Value = 0.144 Expected Conc. = 0.251 Report level label = 0.03 Pct Recovery = 57% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl SpecificMix = 012513 Laboratory ID = 20132420001 Lab Value = 0.153 Expected Conc. = 0.251 Report level label = 0.03 Pct Recovery = 61% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl SpecificMix = 012513 Laboratory ID = 20130940097 Lab Value = 0.067 Expected Conc. = 0.2505 Report level label = 0.03 Pct Recovery = 27% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = 052412 Laboratory ID = 20130100066 Lab Value = 0.122 Expected Conc. = 0.2505 Report level label = 0.03 Pct Recovery = 49% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl SpecificMix = 052412 Laboratory ID = 20172510330 Lab Value = 0.133 Expected Conc. = 0.201 Report level label = 0.03 Pct Recovery = 66% Analysis Date = 12/29/17 SpikeMix = ChemService 6537100: 100 µl & Abs 071817Pest: 100 µl SpecificMix = 071817Pest Laboratory ID = 20162860079 Lab Value = 0.128 Expected Conc. = 0.19 Report level label = 0.03 Pct Recovery = 67% Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl SpecificMix = 5054800 Laboratory ID = 20161880109 Lab Value = 0.181 Expected Conc. = 0.19 Report level label = 0.03 Pct Recovery = 95% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl SpecificMix = 5054800 Laboratory ID = 20163370001 Lab Value = 0.165 Expected Conc. = 0.1875 Report level label = 0.03 Pct Recovery = 88% Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl SpecificMix = LC20138V Laboratory ID = 20132690010 Lab Value = 0.135 Expected Conc. = 0.163 Report level label = 0.03 Pct Recovery = 83% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl SpecificMix = 042413 Laboratory ID = 20132560001 Lab Value = 0.112 Expected Conc. = 0.163 Report level label = 0.03 Pct Recovery = 69% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl SpecificMix = 042413 Laboratory ID = 20132140002 Lab Value = 0.055 Expected Conc. = 0.1595 Report level label = 0.03 Pct Recovery = 34% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl SpecificMix = 04CC101 Laboratory ID = 20171380001 Lab Value = 0.128 Expected Conc. = 0.152 Report level label = 0.03 Pct Recovery = 84% Analysis Date = 06/07/17 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 5054800 Laboratory ID = 20170960001 Lab Value = 0.123 Expected Conc. = 0.152 Report level label = 0.03 Pct Recovery = 81% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl SpecificMix = 5054800 Laboratory ID = 20161740258 Lab Value = 0.123 Expected Conc. = 0.152 Report level label = 0.03 Pct Recovery = 81% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 5054800 Laboratory ID = 20171720140 Lab Value = 0.119 Expected Conc. = 0.15 Report level label = 0.03 Pct Recovery = 79% Analysis Date = 08/31/17 SpikeMix = Supelco LC20138V: 80 µl & Phenova B20160331: 80 µl SpecificMix = LC20138V Laboratory ID = 20170740063 Lab Value = 0.127 Expected Conc. = 0.15 Report level label = 0.03 Pct Recovery = 85% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl SpecificMix = LC20138V Laboratory ID = 20161470001 Lab Value = 0.120 Expected Conc. = 0.15 Report level label = 0.03 Pct Recovery = 80% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl SpecificMix = LC20138V Laboratory ID = 20150720069 Lab Value = 0.102 Expected Conc. = 0.1212 Report level label = 0.03 Pct Recovery = 84% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 0227-14-08 Laboratory ID = 20141770149 Lab Value = 0.104 Expected Conc. = 0.1212 Report level label = 0.03 Pct Recovery = 86% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl SpecificMix = 0227-14-08 Laboratory ID = 20141570088 Lab Value = 0.089 Expected Conc. = 0.1212 Report level label = 0.03 Pct Recovery = 73% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl SpecificMix = 0227-14-08 Laboratory ID = 20150430092 Lab Value = 0.124 Expected Conc. = 0.1206 Report level label = 0.03 Pct Recovery = 103% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl SpecificMix = 042814 Laboratory ID = 20143240095 Lab Value = 0.092 Expected Conc. = 0.1206 Report level label = 0.03 Pct Recovery = 76% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl SpecificMix = 042814 Laboratory ID = 20142960086 Lab Value = 0.102 Expected Conc. = 0.1206 Report level label = 0.03 Pct Recovery = 85% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 042814 Laboratory ID = 20142530087 Lab Value = 0.087 Expected Conc. = 0.1206 Report level label = 0.03 Pct Recovery = 72% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl SpecificMix = 042814 Laboratory ID = 20140860102 Lab Value = 0.077 Expected Conc. = 0.1004 Report level label = 0.03 Pct Recovery = 76% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 012513 Laboratory ID = 20131920149 Lab Value = 0.064 Expected Conc. = 0.1004 Report level label = 0.03 Pct Recovery = 64% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl SpecificMix = 012513 Laboratory ID = 20133400002 Lab Value = 0.068 Expected Conc. = 0.1002 Report level label = 0.03 Pct Recovery = 68% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = 052412 Laboratory ID = 20132910008 Lab Value = 0.090 Expected Conc. = 0.1002 Report level label = 0.03 Pct Recovery = 89% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = 052412 Laboratory ID = 20130650005 Lab Value = 0.058 Expected Conc. = 0.1002 Report level label = 0.03 Pct Recovery = 57% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl SpecificMix = 052412 Laboratory ID = 20172560101 Lab Value = 0.095 Expected Conc. = 0.1 Report level label = 0.03 Pct Recovery = 95% Analysis Date = 12/22/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6567600: 50 µl SpecificMix = 6567600 Laboratory ID = 20131230084 Lab Value = 0.003 Expected Conc. = 0.098 Report level label = 0.03 Pct Recovery = 3% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl SpecificMix = 05BB029 Laboratory ID = 20130510051 Lab Value = 0.056 Expected Conc. = 0.098 Report level label = 0.03 Pct Recovery = 57% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl SpecificMix = 05BB029 Laboratory ID = 20161260151 Lab Value = 0.106 Expected Conc. = 0.092 Report level label = 0.03 Pct Recovery = 115% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = 3851600 Laboratory ID = 20151270112 Lab Value = 0.059 Expected Conc. = 0.092 Report level label = 0.03 Pct Recovery = 65% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl SpecificMix = 3851600 Laboratory ID = 20160770090 Lab Value = 0.076 Expected Conc. = 0.0908 Report level label = 0.03 Pct Recovery = 84% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20160630046 Lab Value = 0.079 Expected Conc. = 0.0908 Report level label = 0.03 Pct Recovery = 86% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20153510109 Lab Value = 0.065 Expected Conc. = 0.0908 Report level label = 0.03 Pct Recovery = 71% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20153440001 Lab Value = 0.064 Expected Conc. = 0.0908 Report level label = 0.03 Pct Recovery = 71% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20171940002 Lab Value = 0.065 Expected Conc. = 0.076 Report level label = 0.03 Pct Recovery = 86% Analysis Date = 11/10/17 SpikeMix = ChemService 5054800: 40 µl & NSI 041816: 40 µl SpecificMix = 5054800 Laboratory ID = 20170460061 Lab Value = 0.066 Expected Conc. = 0.076 Report level label = 0.03 Pct Recovery = 87% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl SpecificMix = 5054800 Laboratory ID = 20163560019 Lab Value = 0.086 Expected Conc. = 0.076 Report level label = 0.03 Pct Recovery = 113% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl SpecificMix = 5054800 Laboratory ID = 20162150213 Lab Value = 0.109 Expected Conc. = 0.076 Report level label = 0.03 Pct Recovery = 143% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl SpecificMix = 5054800 Laboratory ID = 20171510080 Lab Value = 0.066 Expected Conc. = 0.075 Report level label = 0.03 Pct Recovery = 87% Analysis Date = 06/09/17 SpikeMix = Supelco LC20138V: 40 µl & Crescent 03FF076: 40 µl SpecificMix = LC20138V Laboratory ID = 20162520001 Lab Value = 0.080 Expected Conc. = 0.075 Report level label = 0.03 Pct Recovery = 106% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl SpecificMix = LC20138V Laboratory ID = 20162660005 Lab Value = 0.071 Expected Conc. = 0.075 Report level label = 0.03 Pct Recovery = 95% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl SpecificMix = LC20138V Laboratory ID = 20162020124 Lab Value = 0.066 Expected Conc. = 0.075 Report level label = 0.03 Pct Recovery = 87% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl SpecificMix = LC20138V Laboratory ID = 20133580036 Lab Value = 0.045 Expected Conc. = 0.0652 Report level label = 0.03 Pct Recovery = 69% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 042413 Laboratory ID = 20133190012 Lab Value = 0.063 Expected Conc. = 0.0652 Report level label = 0.03 Pct Recovery = 97% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 042413 Laboratory ID = 20131650073 Lab Value = 0.016 Expected Conc. = 0.0652 Report level label = 0.03 Pct Recovery = 25% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl SpecificMix = 042413 Laboratory ID = 20140730138 Lab Value = 0.053 Expected Conc. = 0.0638 Report level label = 0.03 Pct Recovery = 83% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 04CC101 Laboratory ID = 20140510043 Lab Value = 0.064 Expected Conc. = 0.0638 Report level label = 0.03 Pct Recovery = 100% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 04CC101 Laboratory ID = 20133310030 Lab Value = 0.075 Expected Conc. = 0.0638 Report level label = 0.03 Pct Recovery = 118% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl SpecificMix = 04CC101 Laboratory ID = 20132280016 Lab Value = 0.034 Expected Conc. = 0.0638 Report level label = 0.03 Pct Recovery = 53% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl SpecificMix = 04CC101 Laboratory ID = 20131510026 Lab Value = 0.007 Expected Conc. = 0.0638 Report level label = 0.03 Pct Recovery = 11% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl SpecificMix = 04CC101 Laboratory ID = 20141840097 Lab Value = 0.046 Expected Conc. = 0.0606 Report level label = 0.03 Pct Recovery = 76% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20141490205 Lab Value = 0.048 Expected Conc. = 0.0606 Report level label = 0.03 Pct Recovery = 79% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20141420140 Lab Value = 0.037 Expected Conc. = 0.0606 Report level label = 0.03 Pct Recovery = 61% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20141360094 Lab Value = 0.045 Expected Conc. = 0.0606 Report level label = 0.03 Pct Recovery = 75% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20172780018 Lab Value = 0.070 Expected Conc. = 0.0603 Report level label = 0.03 Pct Recovery = 116% Analysis Date = 02/08/18 SpikeMix = ChemService 6537100: 30 µl & Abs 071817Pest: 30 µl SpecificMix = 071817Pest Laboratory ID = 20143370094 Lab Value = 0.055 Expected Conc. = 0.0603 Report level label = 0.03 Pct Recovery = 91% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl SpecificMix = 042814 Laboratory ID = 20142820151 Lab Value = 0.038 Expected Conc. = 0.0603 Report level label = 0.03 Pct Recovery = 63% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl SpecificMix = 042814 Laboratory ID = 20142470041 Lab Value = 0.038 Expected Conc. = 0.0603 Report level label = 0.03 Pct Recovery = 62% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl SpecificMix = 042814 Laboratory ID = 20142200164 Lab Value = 0.038 Expected Conc. = 0.0603 Report level label = 0.03 Pct Recovery = 64% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 042814 Laboratory ID = 20160430111 Lab Value = 0.042 Expected Conc. = 0.046 Report level label = 0.03 Pct Recovery = 91% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 3851600 Laboratory ID = 20160210080 Lab Value = 0.037 Expected Conc. = 0.046 Report level label = 0.03 Pct Recovery = 79% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 3851600 Laboratory ID = 20152950078 Lab Value = 0.037 Expected Conc. = 0.046 Report level label = 0.03 Pct Recovery = 80% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 3851600 Laboratory ID = 20153030068 Lab Value = 0.048 Expected Conc. = 0.046 Report level label = 0.03 Pct Recovery = 103% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = 3851600 Laboratory ID = 20151380009 Lab Value = 0.030 Expected Conc. = 0.046 Report level label = 0.03 Pct Recovery = 65% Analysis Date = 05/30/15 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 3851600 Analysis Date = 02/08/18 Pct Recovery = 92% Analysis Date = 01/29/18 Pct Recovery = 92% Analysis Date = 01/29/18 Pct Recovery = 92% Analysis Date = 01/20/18 Pct Recovery = 91% Analysis Date = 01/20/18 Pct Recovery = 91% Analysis Date = 01/11/18 Pct Recovery = 91% Analysis Date = 01/11/18 Pct Recovery = 91% Analysis Date = 01/02/18 Pct Recovery = 91% Analysis Date = 01/02/18 Pct Recovery = 91% Analysis Date = 12/23/17 Pct Recovery = 91% Analysis Date = 12/23/17 Pct Recovery = 91% Analysis Date = 12/14/17 Pct Recovery = 91% Analysis Date = 12/14/17 Pct Recovery = 91% Analysis Date = 12/05/17 Pct Recovery = 91% Analysis Date = 12/05/17 Pct Recovery = 91% Analysis Date = 11/26/17 Pct Recovery = 91% Analysis Date = 11/26/17 Pct Recovery = 91% Analysis Date = 11/16/17 Pct Recovery = 91% Analysis Date = 11/16/17 Pct Recovery = 91% Analysis Date = 11/07/17 Pct Recovery = 91% Analysis Date = 11/07/17 Pct Recovery = 91% Analysis Date = 10/29/17 Pct Recovery = 91% Analysis Date = 10/29/17 Pct Recovery = 91% Analysis Date = 10/20/17 Pct Recovery = 91% Analysis Date = 10/20/17 Pct Recovery = 91% Analysis Date = 10/10/17 Pct Recovery = 91% Analysis Date = 10/10/17 Pct Recovery = 91% Analysis Date = 10/01/17 Pct Recovery = 91% Analysis Date = 10/01/17 Pct Recovery = 91% Analysis Date = 09/22/17 Pct Recovery = 91% Analysis Date = 09/22/17 Pct Recovery = 91% Analysis Date = 09/13/17 Pct Recovery = 91% Analysis Date = 09/13/17 Pct Recovery = 91% Analysis Date = 09/03/17 Pct Recovery = 91% Analysis Date = 09/03/17 Pct Recovery = 91% Analysis Date = 08/25/17 Pct Recovery = 91% Analysis Date = 08/25/17 Pct Recovery = 91% Analysis Date = 08/16/17 Pct Recovery = 91% Analysis Date = 08/16/17 Pct Recovery = 91% Analysis Date = 08/07/17 Pct Recovery = 91% Analysis Date = 08/07/17 Pct Recovery = 91% Analysis Date = 07/28/17 Pct Recovery = 91% Analysis Date = 07/28/17 Pct Recovery = 91% Analysis Date = 07/19/17 Pct Recovery = 91% Analysis Date = 07/19/17 Pct Recovery = 91% Analysis Date = 07/10/17 Pct Recovery = 91% Analysis Date = 07/10/17 Pct Recovery = 91% Analysis Date = 07/01/17 Pct Recovery = 91% Analysis Date = 07/01/17 Pct Recovery = 91% Analysis Date = 06/22/17 Pct Recovery = 91% Analysis Date = 06/22/17 Pct Recovery = 91% Analysis Date = 06/12/17 Pct Recovery = 91% Analysis Date = 06/12/17 Pct Recovery = 91% Analysis Date = 06/03/17 Pct Recovery = 91% Analysis Date = 06/03/17 Pct Recovery = 91% Analysis Date = 05/25/17 Pct Recovery = 91% Analysis Date = 05/25/17 Pct Recovery = 91% Analysis Date = 05/16/17 Pct Recovery = 90% Analysis Date = 05/16/17 Pct Recovery = 90% Analysis Date = 05/06/17 Pct Recovery = 90% Analysis Date = 05/06/17 Pct Recovery = 90% Analysis Date = 04/27/17 Pct Recovery = 90% Analysis Date = 04/27/17 Pct Recovery = 90% Analysis Date = 04/18/17 Pct Recovery = 90% Analysis Date = 04/18/17 Pct Recovery = 90% Analysis Date = 04/09/17 Pct Recovery = 90% Analysis Date = 04/09/17 Pct Recovery = 90% Analysis Date = 03/30/17 Pct Recovery = 90% Analysis Date = 03/30/17 Pct Recovery = 90% Analysis Date = 03/21/17 Pct Recovery = 90% Analysis Date = 03/21/17 Pct Recovery = 90% Analysis Date = 03/12/17 Pct Recovery = 90% Analysis Date = 03/12/17 Pct Recovery = 90% Analysis Date = 03/03/17 Pct Recovery = 90% Analysis Date = 03/03/17 Pct Recovery = 90% Analysis Date = 02/21/17 Pct Recovery = 90% Analysis Date = 02/21/17 Pct Recovery = 90% Analysis Date = 02/12/17 Pct Recovery = 90% Analysis Date = 02/12/17 Pct Recovery = 90% Analysis Date = 02/03/17 Pct Recovery = 90% Analysis Date = 02/03/17 Pct Recovery = 90% Analysis Date = 01/25/17 Pct Recovery = 90% Analysis Date = 01/25/17 Pct Recovery = 90% Analysis Date = 01/15/17 Pct Recovery = 90% Analysis Date = 01/15/17 Pct Recovery = 90% Analysis Date = 01/06/17 Pct Recovery = 90% Analysis Date = 01/06/17 Pct Recovery = 90% Analysis Date = 12/28/16 Pct Recovery = 90% Analysis Date = 12/28/16 Pct Recovery = 90% Analysis Date = 12/19/16 Pct Recovery = 89% Analysis Date = 12/19/16 Pct Recovery = 89% Analysis Date = 12/09/16 Pct Recovery = 89% Analysis Date = 12/09/16 Pct Recovery = 89% Analysis Date = 11/30/16 Pct Recovery = 89% Analysis Date = 11/30/16 Pct Recovery = 89% Analysis Date = 11/21/16 Pct Recovery = 89% Analysis Date = 11/21/16 Pct Recovery = 89% Analysis Date = 11/12/16 Pct Recovery = 89% Analysis Date = 11/12/16 Pct Recovery = 89% Analysis Date = 11/03/16 Pct Recovery = 89% Analysis Date = 11/03/16 Pct Recovery = 89% Analysis Date = 10/24/16 Pct Recovery = 89% Analysis Date = 10/24/16 Pct Recovery = 89% Analysis Date = 10/15/16 Pct Recovery = 89% Analysis Date = 10/15/16 Pct Recovery = 89% Analysis Date = 10/06/16 Pct Recovery = 89% Analysis Date = 10/06/16 Pct Recovery = 89% Analysis Date = 09/27/16 Pct Recovery = 89% Analysis Date = 09/27/16 Pct Recovery = 89% Analysis Date = 09/17/16 Pct Recovery = 89% Analysis Date = 09/17/16 Pct Recovery = 89% Analysis Date = 09/08/16 Pct Recovery = 89% Analysis Date = 09/08/16 Pct Recovery = 89% Analysis Date = 08/30/16 Pct Recovery = 89% Analysis Date = 08/30/16 Pct Recovery = 89% Analysis Date = 08/21/16 Pct Recovery = 89% Analysis Date = 08/21/16 Pct Recovery = 89% Analysis Date = 08/11/16 Pct Recovery = 88% Analysis Date = 08/11/16 Pct Recovery = 88% Analysis Date = 08/02/16 Pct Recovery = 88% Analysis Date = 08/02/16 Pct Recovery = 88% Analysis Date = 07/24/16 Pct Recovery = 88% Analysis Date = 07/24/16 Pct Recovery = 88% Analysis Date = 07/15/16 Pct Recovery = 88% Analysis Date = 07/15/16 Pct Recovery = 88% Analysis Date = 07/05/16 Pct Recovery = 88% Analysis Date = 07/05/16 Pct Recovery = 88% Analysis Date = 06/26/16 Pct Recovery = 88% Analysis Date = 06/26/16 Pct Recovery = 88% Analysis Date = 06/17/16 Pct Recovery = 88% Analysis Date = 06/17/16 Pct Recovery = 88% Analysis Date = 06/08/16 Pct Recovery = 88% Analysis Date = 06/08/16 Pct Recovery = 88% Analysis Date = 05/29/16 Pct Recovery = 88% Analysis Date = 05/29/16 Pct Recovery = 88% Analysis Date = 05/20/16 Pct Recovery = 88% Analysis Date = 05/20/16 Pct Recovery = 88% Analysis Date = 05/11/16 Pct Recovery = 88% Analysis Date = 05/11/16 Pct Recovery = 88% Analysis Date = 05/02/16 Pct Recovery = 88% Analysis Date = 05/02/16 Pct Recovery = 88% Analysis Date = 04/22/16 Pct Recovery = 87% Analysis Date = 04/22/16 Pct Recovery = 87% Analysis Date = 04/13/16 Pct Recovery = 87% Analysis Date = 04/13/16 Pct Recovery = 87% Analysis Date = 04/04/16 Pct Recovery = 87% Analysis Date = 04/04/16 Pct Recovery = 87% Analysis Date = 03/26/16 Pct Recovery = 87% Analysis Date = 03/26/16 Pct Recovery = 87% Analysis Date = 03/17/16 Pct Recovery = 87% Analysis Date = 03/17/16 Pct Recovery = 87% Analysis Date = 03/07/16 Pct Recovery = 87% Analysis Date = 03/07/16 Pct Recovery = 87% Analysis Date = 02/27/16 Pct Recovery = 87% Analysis Date = 02/27/16 Pct Recovery = 87% Analysis Date = 02/18/16 Pct Recovery = 86% Analysis Date = 02/18/16 Pct Recovery = 86% Analysis Date = 02/09/16 Pct Recovery = 86% Analysis Date = 02/09/16 Pct Recovery = 86% Analysis Date = 01/30/16 Pct Recovery = 86% Analysis Date = 01/30/16 Pct Recovery = 86% Analysis Date = 01/21/16 Pct Recovery = 86% Analysis Date = 01/21/16 Pct Recovery = 86% Analysis Date = 01/12/16 Pct Recovery = 86% Analysis Date = 01/12/16 Pct Recovery = 86% Analysis Date = 01/03/16 Pct Recovery = 85% Analysis Date = 01/03/16 Pct Recovery = 85% Analysis Date = 12/24/15 Pct Recovery = 85% Analysis Date = 12/24/15 Pct Recovery = 85% Analysis Date = 12/15/15 Pct Recovery = 85% Analysis Date = 12/15/15 Pct Recovery = 85% Analysis Date = 12/06/15 Pct Recovery = 85% Analysis Date = 12/06/15 Pct Recovery = 85% Analysis Date = 11/27/15 Pct Recovery = 84% Analysis Date = 11/27/15 Pct Recovery = 84% Analysis Date = 11/17/15 Pct Recovery = 84% Analysis Date = 11/17/15 Pct Recovery = 84% Analysis Date = 11/08/15 Pct Recovery = 84% Analysis Date = 11/08/15 Pct Recovery = 84% Analysis Date = 10/30/15 Pct Recovery = 84% Analysis Date = 10/30/15 Pct Recovery = 84% Analysis Date = 10/21/15 Pct Recovery = 84% Analysis Date = 10/21/15 Pct Recovery = 84% Analysis Date = 10/11/15 Pct Recovery = 83% Analysis Date = 10/11/15 Pct Recovery = 83% Analysis Date = 10/02/15 Pct Recovery = 83% Analysis Date = 10/02/15 Pct Recovery = 83% Analysis Date = 09/23/15 Pct Recovery = 83% Analysis Date = 09/23/15 Pct Recovery = 83% Analysis Date = 09/14/15 Pct Recovery = 83% Analysis Date = 09/14/15 Pct Recovery = 83% Analysis Date = 09/04/15 Pct Recovery = 82% Analysis Date = 09/04/15 Pct Recovery = 82% Analysis Date = 08/26/15 Pct Recovery = 82% Analysis Date = 08/26/15 Pct Recovery = 82% Analysis Date = 08/17/15 Pct Recovery = 82% Analysis Date = 08/17/15 Pct Recovery = 82% Analysis Date = 08/08/15 Pct Recovery = 82% Analysis Date = 08/08/15 Pct Recovery = 82% Analysis Date = 07/30/15 Pct Recovery = 82% Analysis Date = 07/30/15 Pct Recovery = 82% Analysis Date = 07/20/15 Pct Recovery = 81% Analysis Date = 07/20/15 Pct Recovery = 81% Analysis Date = 07/11/15 Pct Recovery = 81% Analysis Date = 07/11/15 Pct Recovery = 81% Analysis Date = 07/02/15 Pct Recovery = 81% Analysis Date = 07/02/15 Pct Recovery = 81% Analysis Date = 06/23/15 Pct Recovery = 81% Analysis Date = 06/23/15 Pct Recovery = 81% Analysis Date = 06/13/15 Pct Recovery = 80% Analysis Date = 06/13/15 Pct Recovery = 80% Analysis Date = 06/04/15 Pct Recovery = 80% Analysis Date = 06/04/15 Pct Recovery = 80% Analysis Date = 05/26/15 Pct Recovery = 80% Analysis Date = 05/26/15 Pct Recovery = 80% Analysis Date = 05/17/15 Pct Recovery = 80% Analysis Date = 05/17/15 Pct Recovery = 80% Analysis Date = 05/07/15 Pct Recovery = 80% Analysis Date = 05/07/15 Pct Recovery = 80% Analysis Date = 04/28/15 Pct Recovery = 79% Analysis Date = 04/28/15 Pct Recovery = 79% Analysis Date = 04/19/15 Pct Recovery = 79% Analysis Date = 04/19/15 Pct Recovery = 79% Analysis Date = 04/10/15 Pct Recovery = 79% Analysis Date = 04/10/15 Pct Recovery = 79% Analysis Date = 03/31/15 Pct Recovery = 79% Analysis Date = 03/31/15 Pct Recovery = 79% Analysis Date = 03/22/15 Pct Recovery = 79% Analysis Date = 03/22/15 Pct Recovery = 79% Analysis Date = 03/13/15 Pct Recovery = 79% Analysis Date = 03/13/15 Pct Recovery = 79% Analysis Date = 03/04/15 Pct Recovery = 79% Analysis Date = 03/04/15 Pct Recovery = 79% Analysis Date = 02/22/15 Pct Recovery = 78% Analysis Date = 02/22/15 Pct Recovery = 78% Analysis Date = 02/13/15 Pct Recovery = 78% Analysis Date = 02/13/15 Pct Recovery = 78% Analysis Date = 02/04/15 Pct Recovery = 78% Analysis Date = 02/04/15 Pct Recovery = 78% Analysis Date = 01/26/15 Pct Recovery = 78% Analysis Date = 01/26/15 Pct Recovery = 78% Analysis Date = 01/16/15 Pct Recovery = 78% Analysis Date = 01/16/15 Pct Recovery = 78% Analysis Date = 01/07/15 Pct Recovery = 78% Analysis Date = 01/07/15 Pct Recovery = 78% Analysis Date = 12/29/14 Pct Recovery = 78% Analysis Date = 12/29/14 Pct Recovery = 78% Analysis Date = 12/20/14 Pct Recovery = 77% Analysis Date = 12/20/14 Pct Recovery = 77% Analysis Date = 12/11/14 Pct Recovery = 77% Analysis Date = 12/11/14 Pct Recovery = 77% Analysis Date = 12/01/14 Pct Recovery = 77% Analysis Date = 12/01/14 Pct Recovery = 77% Analysis Date = 11/22/14 Pct Recovery = 77% Analysis Date = 11/22/14 Pct Recovery = 77% Analysis Date = 11/13/14 Pct Recovery = 77% Analysis Date = 11/13/14 Pct Recovery = 77% Analysis Date = 11/04/14 Pct Recovery = 77% Analysis Date = 11/04/14 Pct Recovery = 77% Analysis Date = 10/25/14 Pct Recovery = 76% Analysis Date = 10/25/14 Pct Recovery = 76% Analysis Date = 10/16/14 Pct Recovery = 76% Analysis Date = 10/16/14 Pct Recovery = 76% Analysis Date = 10/07/14 Pct Recovery = 76% Analysis Date = 10/07/14 Pct Recovery = 76% Analysis Date = 09/28/14 Pct Recovery = 76% Analysis Date = 09/28/14 Pct Recovery = 76% Analysis Date = 09/18/14 Pct Recovery = 76% Analysis Date = 09/18/14 Pct Recovery = 76% Analysis Date = 09/09/14 Pct Recovery = 76% Analysis Date = 09/09/14 Pct Recovery = 76% Analysis Date = 08/31/14 Pct Recovery = 76% Analysis Date = 08/31/14 Pct Recovery = 76% Analysis Date = 08/22/14 Pct Recovery = 76% Analysis Date = 08/22/14 Pct Recovery = 76% Analysis Date = 08/12/14 Pct Recovery = 75% Analysis Date = 08/12/14 Pct Recovery = 75% Analysis Date = 08/03/14 Pct Recovery = 75% Analysis Date = 08/03/14 Pct Recovery = 75% Analysis Date = 07/25/14 Pct Recovery = 75% Analysis Date = 07/25/14 Pct Recovery = 75% Analysis Date = 07/16/14 Pct Recovery = 75% Analysis Date = 07/16/14 Pct Recovery = 75% Analysis Date = 07/06/14 Pct Recovery = 75% Analysis Date = 07/06/14 Pct Recovery = 75% Analysis Date = 06/27/14 Pct Recovery = 75% Analysis Date = 06/27/14 Pct Recovery = 75% Analysis Date = 06/18/14 Pct Recovery = 74% Analysis Date = 06/18/14 Pct Recovery = 74% Analysis Date = 06/09/14 Pct Recovery = 74% Analysis Date = 06/09/14 Pct Recovery = 74% Analysis Date = 05/30/14 Pct Recovery = 73% Analysis Date = 05/30/14 Pct Recovery = 73% Analysis Date = 05/21/14 Pct Recovery = 73% Analysis Date = 05/21/14 Pct Recovery = 73% Analysis Date = 05/12/14 Pct Recovery = 72% Analysis Date = 05/12/14 Pct Recovery = 72% Analysis Date = 05/03/14 Pct Recovery = 72% Analysis Date = 05/03/14 Pct Recovery = 72% Analysis Date = 04/24/14 Pct Recovery = 71% Analysis Date = 04/24/14 Pct Recovery = 71% Analysis Date = 04/14/14 Pct Recovery = 71% Analysis Date = 04/14/14 Pct Recovery = 71% Analysis Date = 04/05/14 Pct Recovery = 70% Analysis Date = 04/05/14 Pct Recovery = 70% Analysis Date = 03/27/14 Pct Recovery = 70% Analysis Date = 03/27/14 Pct Recovery = 70% Analysis Date = 03/18/14 Pct Recovery = 69% Analysis Date = 03/18/14 Pct Recovery = 69% Analysis Date = 03/08/14 Pct Recovery = 69% Analysis Date = 03/08/14 Pct Recovery = 69% Analysis Date = 02/27/14 Pct Recovery = 68% Analysis Date = 02/27/14 Pct Recovery = 68% Analysis Date = 02/18/14 Pct Recovery = 68% Analysis Date = 02/18/14 Pct Recovery = 68% Analysis Date = 02/09/14 Pct Recovery = 67% Analysis Date = 02/09/14 Pct Recovery = 67% Analysis Date = 01/30/14 Pct Recovery = 67% Analysis Date = 01/30/14 Pct Recovery = 67% Analysis Date = 01/21/14 Pct Recovery = 66% Analysis Date = 01/21/14 Pct Recovery = 66% Analysis Date = 01/12/14 Pct Recovery = 65% Analysis Date = 01/12/14 Pct Recovery = 65% Analysis Date = 01/03/14 Pct Recovery = 65% Analysis Date = 01/03/14 Pct Recovery = 65% Analysis Date = 12/24/13 Pct Recovery = 64% Analysis Date = 12/24/13 Pct Recovery = 64% Analysis Date = 12/15/13 Pct Recovery = 64% Analysis Date = 12/15/13 Pct Recovery = 64% Analysis Date = 12/06/13 Pct Recovery = 63% Analysis Date = 12/06/13 Pct Recovery = 63% Analysis Date = 11/27/13 Pct Recovery = 63% Analysis Date = 11/27/13 Pct Recovery = 63% Analysis Date = 11/17/13 Pct Recovery = 62% Analysis Date = 11/17/13 Pct Recovery = 62% Analysis Date = 11/08/13 Pct Recovery = 62% Analysis Date = 11/08/13 Pct Recovery = 62% Analysis Date = 10/30/13 Pct Recovery = 61% Analysis Date = 10/30/13 Pct Recovery = 61% Analysis Date = 10/21/13 Pct Recovery = 60% Analysis Date = 10/21/13 Pct Recovery = 60% Analysis Date = 10/11/13 Pct Recovery = 60% Analysis Date = 10/11/13 Pct Recovery = 60% Analysis Date = 10/02/13 Pct Recovery = 59% Analysis Date = 10/02/13 Pct Recovery = 59% Analysis Date = 09/23/13 Pct Recovery = 59% Analysis Date = 09/23/13 Pct Recovery = 59% Analysis Date = 09/14/13 Pct Recovery = 58% Analysis Date = 09/14/13 Pct Recovery = 58% Analysis Date = 09/05/13 Pct Recovery = 58% Analysis Date = 09/05/13 Pct Recovery = 58% Analysis Date = 08/26/13 Pct Recovery = 57% Analysis Date = 08/26/13 Pct Recovery = 57% Analysis Date = 08/17/13 Pct Recovery = 56% Analysis Date = 08/17/13 Pct Recovery = 56% Analysis Date = 08/08/13 Pct Recovery = 56% Analysis Date = 08/08/13 Pct Recovery = 56% Analysis Date = 07/30/13 Pct Recovery = 55% Analysis Date = 07/30/13 Pct Recovery = 55% Analysis Date = 07/20/13 Pct Recovery = 55% Analysis Date = 07/20/13 Pct Recovery = 55% Analysis Date = 07/11/13 Pct Recovery = 54% Analysis Date = 07/11/13 Pct Recovery = 54% Analysis Date = 07/02/13 Pct Recovery = 53% Analysis Date = 07/02/13 Pct Recovery = 53% Analysis Date = 06/23/13 Pct Recovery = 53% Analysis Date = 06/23/13 Pct Recovery = 53% Analysis Date = 06/13/13 Pct Recovery = 52% Analysis Date = 06/13/13 Pct Recovery = 52% Analysis Date = 06/04/13 Pct Recovery = 52% Analysis Date = 06/04/13 Pct Recovery = 52% Analysis Date = 05/26/13 Pct Recovery = 51% Analysis Date = 05/26/13 Pct Recovery = 51% Analysis Date = 05/17/13 Pct Recovery = 50% Analysis Date = 05/17/13 Pct Recovery = 50% Analysis Date = 05/07/13 Pct Recovery = 50% Analysis Date = 05/07/13 Pct Recovery = 50% Analysis Date = 04/28/13 Pct Recovery = 49% Analysis Date = 04/28/13 Pct Recovery = 49% Analysis Date = 04/19/13 Pct Recovery = 49% Analysis Date = 04/19/13 Pct Recovery = 49% Analysis Date = 04/10/13 Pct Recovery = 48% Analysis Date = 04/10/13 Pct Recovery = 48% Analysis Date = 03/31/13 Pct Recovery = 47% Analysis Date = 03/31/13 Pct Recovery = 47% Analysis Date = 03/22/13 Pct Recovery = 47% Analysis Date = 03/22/13 Pct Recovery = 47% Analysis Date = 03/13/13 Pct Recovery = 46% Analysis Date = 03/13/13 Pct Recovery = 46% Analysis Date = 03/04/13 Pct Recovery = 45% Analysis Date = 03/04/13 Pct Recovery = 45% Analysis Date = 02/22/13 Pct Recovery = 45% Analysis Date = 02/22/13 Pct Recovery = 45% Analysis Date = 02/13/13 Pct Recovery = 44% Analysis Date = 02/13/13 Pct Recovery = 44% Analysis Date = 02/04/13 Pct Recovery = 43% Analysis Date = 02/04/13 Pct Recovery = 43% Analysis Date = 01/26/13 Pct Recovery = 43% Analysis Date = 01/26/13 Pct Recovery = 43% Analysis Date = 01/17/13 Pct Recovery = 42% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
FENAMIPHOS

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 70 76% 24% 79% 17%
Total 70 76% 24% 79% 17%

Sample Statistics
FENAMIPHOS

Characteristic N % % Basis
Plotted 70 96% Spiked
Estimated Values 0 0% Spiked
Deleted Values 4 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 76 .  
False Negatives 3 4% 3 out of 73
Not Spiked 42 .  
False Positives 1 2% 1 out of 41

OBSP Determination:
FENAMIPHOS SULFONE
METHOD: 2033 , TESTIDCODE: 61645GCM39

Laboratory ID = 20140100085 Lab Value = 0.286 Expected Conc. = 0.401 Report level label = 0.054 Pct Recovery = 71% Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl SpecificMix = 042413 Laboratory ID = 20172510330 Lab Value = 0.213 Expected Conc. = 0.361 Report level label = 0.054 Pct Recovery = 59% Analysis Date = 12/29/17 SpikeMix = ChemService 6537100: 100 µl & Abs 071817Pest: 100 µl SpecificMix = 071817Pest Laboratory ID = 20163370001 Lab Value = 0.217 Expected Conc. = 0.3375 Report level label = 0.054 Pct Recovery = 64% Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl SpecificMix = LC20138V Laboratory ID = 20162860079 Lab Value = 0.211 Expected Conc. = 0.33 Report level label = 0.054 Pct Recovery = 64% Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl SpecificMix = 5054800 Laboratory ID = 20161880109 Lab Value = 0.260 Expected Conc. = 0.33 Report level label = 0.054 Pct Recovery = 79% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl SpecificMix = 5054800 Laboratory ID = 20152610011 Lab Value = 0.224 Expected Conc. = 0.3224 Report level label = 0.054 Pct Recovery = 69% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl SpecificMix = 0406-15-01 Laboratory ID = 20152460215 Lab Value = 0.262 Expected Conc. = 0.3224 Report level label = 0.054 Pct Recovery = 81% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl SpecificMix = 0406-15-01 Laboratory ID = 20130250061 Lab Value = 0.194 Expected Conc. = 0.296 Report level label = 0.054 Pct Recovery = 66% Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl SpecificMix = 05BB029 Laboratory ID = 20171720140 Lab Value = 0.146 Expected Conc. = 0.27 Report level label = 0.054 Pct Recovery = 54% Analysis Date = 08/31/17 SpikeMix = Supelco LC20138V: 80 µl & Phenova B20160331: 80 µl SpecificMix = LC20138V Laboratory ID = 20170740063 Lab Value = 0.098 Expected Conc. = 0.27 Report level label = 0.054 Pct Recovery = 36% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl SpecificMix = LC20138V Laboratory ID = 20161470001 Lab Value = 0.183 Expected Conc. = 0.27 Report level label = 0.054 Pct Recovery = 68% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl SpecificMix = LC20138V Laboratory ID = 20171380001 Lab Value = 0.162 Expected Conc. = 0.264 Report level label = 0.054 Pct Recovery = 61% Analysis Date = 06/07/17 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 5054800 Laboratory ID = 20170960001 Lab Value = 0.178 Expected Conc. = 0.264 Report level label = 0.054 Pct Recovery = 67% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl SpecificMix = 5054800 Laboratory ID = 20161740258 Lab Value = 0.187 Expected Conc. = 0.264 Report level label = 0.054 Pct Recovery = 71% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 5054800 Laboratory ID = 20150430092 Lab Value = 0.092 Expected Conc. = 0.2166 Report level label = 0.054 Pct Recovery = 43% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl SpecificMix = 042814 Laboratory ID = 20143240095 Lab Value = 0.127 Expected Conc. = 0.2166 Report level label = 0.054 Pct Recovery = 59% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl SpecificMix = 042814 Laboratory ID = 20142960086 Lab Value = 0.127 Expected Conc. = 0.2166 Report level label = 0.054 Pct Recovery = 59% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 042814 Laboratory ID = 20142530087 Lab Value = 0.087 Expected Conc. = 0.2166 Report level label = 0.054 Pct Recovery = 40% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl SpecificMix = 042814 Laboratory ID = 20150720069 Lab Value = 0.080 Expected Conc. = 0.2148 Report level label = 0.054 Pct Recovery = 37% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 0227-14-08 Laboratory ID = 20141770149 Lab Value = 0.146 Expected Conc. = 0.2148 Report level label = 0.054 Pct Recovery = 68% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl SpecificMix = 0227-14-08 Laboratory ID = 20141570088 Lab Value = 0.156 Expected Conc. = 0.2148 Report level label = 0.054 Pct Recovery = 73% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl SpecificMix = 0227-14-08 Laboratory ID = 20132690010 Lab Value = 0.141 Expected Conc. = 0.2005 Report level label = 0.054 Pct Recovery = 70% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl SpecificMix = 042413 Laboratory ID = 20132560001 Lab Value = 0.121 Expected Conc. = 0.2005 Report level label = 0.054 Pct Recovery = 60% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl SpecificMix = 042413 Laboratory ID = 20132140002 Lab Value = 0.107 Expected Conc. = 0.197 Report level label = 0.054 Pct Recovery = 54% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl SpecificMix = 04CC101 Laboratory ID = 20172560101 Lab Value = 0.161 Expected Conc. = 0.18 Report level label = 0.054 Pct Recovery = 89% Analysis Date = 12/22/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6567600: 50 µl SpecificMix = 6567600 Laboratory ID = 20160770090 Lab Value = 0.134 Expected Conc. = 0.1612 Report level label = 0.054 Pct Recovery = 83% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20160630046 Lab Value = 0.141 Expected Conc. = 0.1612 Report level label = 0.054 Pct Recovery = 87% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20153510109 Lab Value = 0.095 Expected Conc. = 0.1612 Report level label = 0.054 Pct Recovery = 59% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20153440001 Lab Value = 0.101 Expected Conc. = 0.1612 Report level label = 0.054 Pct Recovery = 63% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20161260151 Lab Value = 0.146 Expected Conc. = 0.16 Report level label = 0.054 Pct Recovery = 91% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = 3851600 Laboratory ID = 20151550293 Lab Value = 0.103 Expected Conc. = 0.16 Report level label = 0.054 Pct Recovery = 64% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl SpecificMix = 3851600 Laboratory ID = 20151270112 Lab Value = 0.092 Expected Conc. = 0.16 Report level label = 0.054 Pct Recovery = 58% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl SpecificMix = 3851600 Laboratory ID = 20140230082 Lab Value = 0.115 Expected Conc. = 0.1505 Report level label = 0.054 Pct Recovery = 76% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl SpecificMix = 012513 Laboratory ID = 20132420001 Lab Value = 0.121 Expected Conc. = 0.1505 Report level label = 0.054 Pct Recovery = 80% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl SpecificMix = 012513 Laboratory ID = 20130940097 Lab Value = 0.112 Expected Conc. = 0.15 Report level label = 0.054 Pct Recovery = 75% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = 052412 Laboratory ID = 20130100066 Lab Value = 0.138 Expected Conc. = 0.15 Report level label = 0.054 Pct Recovery = 92% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl SpecificMix = 052412 Laboratory ID = 20171510080 Lab Value = 0.111 Expected Conc. = 0.135 Report level label = 0.054 Pct Recovery = 82% Analysis Date = 06/09/17 SpikeMix = Supelco LC20138V: 40 µl & Crescent 03FF076: 40 µl SpecificMix = LC20138V Laboratory ID = 20162520001 Lab Value = 0.140 Expected Conc. = 0.135 Report level label = 0.054 Pct Recovery = 104% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl SpecificMix = LC20138V Laboratory ID = 20162660005 Lab Value = 0.115 Expected Conc. = 0.135 Report level label = 0.054 Pct Recovery = 85% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl SpecificMix = LC20138V Laboratory ID = 20162020124 Lab Value = 0.099 Expected Conc. = 0.135 Report level label = 0.054 Pct Recovery = 73% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl SpecificMix = LC20138V Laboratory ID = 20171940002 Lab Value = 0.094 Expected Conc. = 0.132 Report level label = 0.054 Pct Recovery = 71% Analysis Date = 11/10/17 SpikeMix = ChemService 5054800: 40 µl & NSI 041816: 40 µl SpecificMix = 5054800 Laboratory ID = 20170460061 Lab Value = 0.106 Expected Conc. = 0.132 Report level label = 0.054 Pct Recovery = 80% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl SpecificMix = 5054800 Laboratory ID = 20163560019 Lab Value = 0.127 Expected Conc. = 0.132 Report level label = 0.054 Pct Recovery = 96% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl SpecificMix = 5054800 Laboratory ID = 20162150213 Lab Value = 0.126 Expected Conc. = 0.132 Report level label = 0.054 Pct Recovery = 95% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl SpecificMix = 5054800 Laboratory ID = 20172780018 Lab Value = 0.129 Expected Conc. = 0.1083 Report level label = 0.054 Pct Recovery = 119% Analysis Date = 02/08/18 SpikeMix = ChemService 6537100: 30 µl & Abs 071817Pest: 30 µl SpecificMix = 071817Pest Laboratory ID = 20143370094 Lab Value = 0.076 Expected Conc. = 0.1083 Report level label = 0.054 Pct Recovery = 70% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl SpecificMix = 042814 Laboratory ID = 20142820151 Lab Value = 0.103 Expected Conc. = 0.1083 Report level label = 0.054 Pct Recovery = 95% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl SpecificMix = 042814 Laboratory ID = 20142470041 Lab Value = 0.075 Expected Conc. = 0.1083 Report level label = 0.054 Pct Recovery = 69% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl SpecificMix = 042814 Laboratory ID = 20142200164 Lab Value = 0.074 Expected Conc. = 0.1083 Report level label = 0.054 Pct Recovery = 69% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 042814 Laboratory ID = 20141840097 Lab Value = 0.059 Expected Conc. = 0.1074 Report level label = 0.054 Pct Recovery = 54% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20141490205 Lab Value = 0.080 Expected Conc. = 0.1074 Report level label = 0.054 Pct Recovery = 75% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20141420140 Lab Value = 0.095 Expected Conc. = 0.1074 Report level label = 0.054 Pct Recovery = 89% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20141360094 Lab Value = 0.047 Expected Conc. = 0.1074 Report level label = 0.054 Pct Recovery = 44% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20152190003 Lab Value = 0.078 Expected Conc. = 0.0806 Report level label = 0.054 Pct Recovery = 97% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = 0406-15-01 Laboratory ID = 20152040177 Lab Value = 0.042 Expected Conc. = 0.0806 Report level label = 0.054 Pct Recovery = 52% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl SpecificMix = 0406-15-01 Laboratory ID = 20133580036 Lab Value = 0.061 Expected Conc. = 0.0802 Report level label = 0.054 Pct Recovery = 76% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 042413 Laboratory ID = 20133190012 Lab Value = 0.106 Expected Conc. = 0.0802 Report level label = 0.054 Pct Recovery = 132% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 042413 Laboratory ID = 20131650073 Lab Value = 0.081 Expected Conc. = 0.0802 Report level label = 0.054 Pct Recovery = 101% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl SpecificMix = 042413 Laboratory ID = 20160430111 Lab Value = 0.077 Expected Conc. = 0.08 Report level label = 0.054 Pct Recovery = 96% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 3851600 Laboratory ID = 20160210080 Lab Value = 0.065 Expected Conc. = 0.08 Report level label = 0.054 Pct Recovery = 81% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 3851600 Laboratory ID = 20152950078 Lab Value = 0.053 Expected Conc. = 0.08 Report level label = 0.054 Pct Recovery = 66% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 3851600 Laboratory ID = 20153030068 Lab Value = 0.067 Expected Conc. = 0.08 Report level label = 0.054 Pct Recovery = 84% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = 3851600 Laboratory ID = 20151760208 Lab Value = 0.068 Expected Conc. = 0.08 Report level label = 0.054 Pct Recovery = 85% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl SpecificMix = 3851600 Laboratory ID = 20151380009 Lab Value = 0.066 Expected Conc. = 0.08 Report level label = 0.054 Pct Recovery = 82% Analysis Date = 05/30/15 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 3851600 Laboratory ID = 20140730138 Lab Value = 0.038 Expected Conc. = 0.0788 Report level label = 0.054 Pct Recovery = 48% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 04CC101 Laboratory ID = 20140510043 Lab Value = 0.064 Expected Conc. = 0.0788 Report level label = 0.054 Pct Recovery = 81% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 04CC101 Laboratory ID = 20133310030 Lab Value = 0.126 Expected Conc. = 0.0788 Report level label = 0.054 Pct Recovery = 160% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl SpecificMix = 04CC101 Laboratory ID = 20132280016 Lab Value = 0.085 Expected Conc. = 0.0788 Report level label = 0.054 Pct Recovery = 108% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl SpecificMix = 04CC101 Laboratory ID = 20131510026 Lab Value = 0.095 Expected Conc. = 0.0788 Report level label = 0.054 Pct Recovery = 121% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl SpecificMix = 04CC101 Laboratory ID = 20140860102 Lab Value = 0.050 Expected Conc. = 0.0602 Report level label = 0.054 Pct Recovery = 82% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 012513 Laboratory ID = 20131920149 Lab Value = 0.058 Expected Conc. = 0.0602 Report level label = 0.054 Pct Recovery = 97% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl SpecificMix = 012513 Laboratory ID = 20133400002 Lab Value = 0.053 Expected Conc. = 0.06 Report level label = 0.054 Pct Recovery = 88% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = 052412 Laboratory ID = 20132910008 Lab Value = 0.047 Expected Conc. = 0.06 Report level label = 0.054 Pct Recovery = 79% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = 052412 Laboratory ID = 20130650005 Lab Value = 0.047 Expected Conc. = 0.06 Report level label = 0.054 Pct Recovery = 79% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl SpecificMix = 052412 Laboratory ID = 20131230084 Lab Value = 0.071 Expected Conc. = 0.0592 Report level label = 0.054 Pct Recovery = 120% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl SpecificMix = 05BB029 Laboratory ID = 20130510051 Lab Value = 0.064 Expected Conc. = 0.0592 Report level label = 0.054 Pct Recovery = 108% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl SpecificMix = 05BB029 Analysis Date = 02/08/18 Pct Recovery = 78% Analysis Date = 01/29/18 Pct Recovery = 78% Analysis Date = 01/29/18 Pct Recovery = 78% Analysis Date = 01/20/18 Pct Recovery = 78% Analysis Date = 01/20/18 Pct Recovery = 78% Analysis Date = 01/11/18 Pct Recovery = 78% Analysis Date = 01/11/18 Pct Recovery = 78% Analysis Date = 01/02/18 Pct Recovery = 78% Analysis Date = 01/02/18 Pct Recovery = 78% Analysis Date = 12/23/17 Pct Recovery = 78% Analysis Date = 12/23/17 Pct Recovery = 78% Analysis Date = 12/14/17 Pct Recovery = 78% Analysis Date = 12/14/17 Pct Recovery = 78% Analysis Date = 12/05/17 Pct Recovery = 78% Analysis Date = 12/05/17 Pct Recovery = 78% Analysis Date = 11/26/17 Pct Recovery = 78% Analysis Date = 11/26/17 Pct Recovery = 78% Analysis Date = 11/16/17 Pct Recovery = 78% Analysis Date = 11/16/17 Pct Recovery = 78% Analysis Date = 11/07/17 Pct Recovery = 78% Analysis Date = 11/07/17 Pct Recovery = 78% Analysis Date = 10/29/17 Pct Recovery = 78% Analysis Date = 10/29/17 Pct Recovery = 78% Analysis Date = 10/20/17 Pct Recovery = 78% Analysis Date = 10/20/17 Pct Recovery = 78% Analysis Date = 10/10/17 Pct Recovery = 78% Analysis Date = 10/10/17 Pct Recovery = 78% Analysis Date = 10/01/17 Pct Recovery = 78% Analysis Date = 10/01/17 Pct Recovery = 78% Analysis Date = 09/22/17 Pct Recovery = 78% Analysis Date = 09/22/17 Pct Recovery = 78% Analysis Date = 09/13/17 Pct Recovery = 78% Analysis Date = 09/13/17 Pct Recovery = 78% Analysis Date = 09/03/17 Pct Recovery = 77% Analysis Date = 09/03/17 Pct Recovery = 77% Analysis Date = 08/25/17 Pct Recovery = 77% Analysis Date = 08/25/17 Pct Recovery = 77% Analysis Date = 08/16/17 Pct Recovery = 77% Analysis Date = 08/16/17 Pct Recovery = 77% Analysis Date = 08/07/17 Pct Recovery = 77% Analysis Date = 08/07/17 Pct Recovery = 77% Analysis Date = 07/28/17 Pct Recovery = 77% Analysis Date = 07/28/17 Pct Recovery = 77% Analysis Date = 07/19/17 Pct Recovery = 77% Analysis Date = 07/19/17 Pct Recovery = 77% Analysis Date = 07/10/17 Pct Recovery = 77% Analysis Date = 07/10/17 Pct Recovery = 77% Analysis Date = 07/01/17 Pct Recovery = 77% Analysis Date = 07/01/17 Pct Recovery = 77% Analysis Date = 06/22/17 Pct Recovery = 77% Analysis Date = 06/22/17 Pct Recovery = 77% Analysis Date = 06/12/17 Pct Recovery = 77% Analysis Date = 06/12/17 Pct Recovery = 77% Analysis Date = 06/03/17 Pct Recovery = 77% Analysis Date = 06/03/17 Pct Recovery = 77% Analysis Date = 05/25/17 Pct Recovery = 77% Analysis Date = 05/25/17 Pct Recovery = 77% Analysis Date = 05/16/17 Pct Recovery = 77% Analysis Date = 05/16/17 Pct Recovery = 77% Analysis Date = 05/06/17 Pct Recovery = 77% Analysis Date = 05/06/17 Pct Recovery = 77% Analysis Date = 04/27/17 Pct Recovery = 77% Analysis Date = 04/27/17 Pct Recovery = 77% Analysis Date = 04/18/17 Pct Recovery = 77% Analysis Date = 04/18/17 Pct Recovery = 77% Analysis Date = 04/09/17 Pct Recovery = 77% Analysis Date = 04/09/17 Pct Recovery = 77% Analysis Date = 03/30/17 Pct Recovery = 77% Analysis Date = 03/30/17 Pct Recovery = 77% Analysis Date = 03/21/17 Pct Recovery = 77% Analysis Date = 03/21/17 Pct Recovery = 77% Analysis Date = 03/12/17 Pct Recovery = 77% Analysis Date = 03/12/17 Pct Recovery = 77% Analysis Date = 03/03/17 Pct Recovery = 77% Analysis Date = 03/03/17 Pct Recovery = 77% Analysis Date = 02/21/17 Pct Recovery = 77% Analysis Date = 02/21/17 Pct Recovery = 77% Analysis Date = 02/12/17 Pct Recovery = 77% Analysis Date = 02/12/17 Pct Recovery = 77% Analysis Date = 02/03/17 Pct Recovery = 77% Analysis Date = 02/03/17 Pct Recovery = 77% Analysis Date = 01/25/17 Pct Recovery = 77% Analysis Date = 01/25/17 Pct Recovery = 77% Analysis Date = 01/15/17 Pct Recovery = 76% Analysis Date = 01/15/17 Pct Recovery = 76% Analysis Date = 01/06/17 Pct Recovery = 76% Analysis Date = 01/06/17 Pct Recovery = 76% Analysis Date = 12/28/16 Pct Recovery = 76% Analysis Date = 12/28/16 Pct Recovery = 76% Analysis Date = 12/19/16 Pct Recovery = 76% Analysis Date = 12/19/16 Pct Recovery = 76% Analysis Date = 12/09/16 Pct Recovery = 76% Analysis Date = 12/09/16 Pct Recovery = 76% Analysis Date = 11/30/16 Pct Recovery = 76% Analysis Date = 11/30/16 Pct Recovery = 76% Analysis Date = 11/21/16 Pct Recovery = 76% Analysis Date = 11/21/16 Pct Recovery = 76% Analysis Date = 11/12/16 Pct Recovery = 76% Analysis Date = 11/12/16 Pct Recovery = 76% Analysis Date = 11/03/16 Pct Recovery = 76% Analysis Date = 11/03/16 Pct Recovery = 76% Analysis Date = 10/24/16 Pct Recovery = 76% Analysis Date = 10/24/16 Pct Recovery = 76% Analysis Date = 10/15/16 Pct Recovery = 76% Analysis Date = 10/15/16 Pct Recovery = 76% Analysis Date = 10/06/16 Pct Recovery = 76% Analysis Date = 10/06/16 Pct Recovery = 76% Analysis Date = 09/27/16 Pct Recovery = 76% Analysis Date = 09/27/16 Pct Recovery = 76% Analysis Date = 09/17/16 Pct Recovery = 76% Analysis Date = 09/17/16 Pct Recovery = 76% Analysis Date = 09/08/16 Pct Recovery = 76% Analysis Date = 09/08/16 Pct Recovery = 76% Analysis Date = 08/30/16 Pct Recovery = 76% Analysis Date = 08/30/16 Pct Recovery = 76% Analysis Date = 08/21/16 Pct Recovery = 76% Analysis Date = 08/21/16 Pct Recovery = 76% Analysis Date = 08/11/16 Pct Recovery = 76% Analysis Date = 08/11/16 Pct Recovery = 76% Analysis Date = 08/02/16 Pct Recovery = 76% Analysis Date = 08/02/16 Pct Recovery = 76% Analysis Date = 07/24/16 Pct Recovery = 75% Analysis Date = 07/24/16 Pct Recovery = 75% Analysis Date = 07/15/16 Pct Recovery = 75% Analysis Date = 07/15/16 Pct Recovery = 75% Analysis Date = 07/05/16 Pct Recovery = 75% Analysis Date = 07/05/16 Pct Recovery = 75% Analysis Date = 06/26/16 Pct Recovery = 75% Analysis Date = 06/26/16 Pct Recovery = 75% Analysis Date = 06/17/16 Pct Recovery = 75% Analysis Date = 06/17/16 Pct Recovery = 75% Analysis Date = 06/08/16 Pct Recovery = 75% Analysis Date = 06/08/16 Pct Recovery = 75% Analysis Date = 05/29/16 Pct Recovery = 75% Analysis Date = 05/29/16 Pct Recovery = 75% Analysis Date = 05/20/16 Pct Recovery = 75% Analysis Date = 05/20/16 Pct Recovery = 75% Analysis Date = 05/11/16 Pct Recovery = 75% Analysis Date = 05/11/16 Pct Recovery = 75% Analysis Date = 05/02/16 Pct Recovery = 75% Analysis Date = 05/02/16 Pct Recovery = 75% Analysis Date = 04/22/16 Pct Recovery = 75% Analysis Date = 04/22/16 Pct Recovery = 75% Analysis Date = 04/13/16 Pct Recovery = 75% Analysis Date = 04/13/16 Pct Recovery = 75% Analysis Date = 04/04/16 Pct Recovery = 75% Analysis Date = 04/04/16 Pct Recovery = 75% Analysis Date = 03/26/16 Pct Recovery = 75% Analysis Date = 03/26/16 Pct Recovery = 75% Analysis Date = 03/17/16 Pct Recovery = 75% Analysis Date = 03/17/16 Pct Recovery = 75% Analysis Date = 03/07/16 Pct Recovery = 75% Analysis Date = 03/07/16 Pct Recovery = 75% Analysis Date = 02/27/16 Pct Recovery = 75% Analysis Date = 02/27/16 Pct Recovery = 75% Analysis Date = 02/18/16 Pct Recovery = 75% Analysis Date = 02/18/16 Pct Recovery = 75% Analysis Date = 02/09/16 Pct Recovery = 74% Analysis Date = 02/09/16 Pct Recovery = 74% Analysis Date = 01/30/16 Pct Recovery = 74% Analysis Date = 01/30/16 Pct Recovery = 74% Analysis Date = 01/21/16 Pct Recovery = 74% Analysis Date = 01/21/16 Pct Recovery = 74% Analysis Date = 01/12/16 Pct Recovery = 74% Analysis Date = 01/12/16 Pct Recovery = 74% Analysis Date = 01/03/16 Pct Recovery = 74% Analysis Date = 01/03/16 Pct Recovery = 74% Analysis Date = 12/24/15 Pct Recovery = 74% Analysis Date = 12/24/15 Pct Recovery = 74% Analysis Date = 12/15/15 Pct Recovery = 74% Analysis Date = 12/15/15 Pct Recovery = 74% Analysis Date = 12/06/15 Pct Recovery = 73% Analysis Date = 12/06/15 Pct Recovery = 73% Analysis Date = 11/27/15 Pct Recovery = 73% Analysis Date = 11/27/15 Pct Recovery = 73% Analysis Date = 11/17/15 Pct Recovery = 73% Analysis Date = 11/17/15 Pct Recovery = 73% Analysis Date = 11/08/15 Pct Recovery = 73% Analysis Date = 11/08/15 Pct Recovery = 73% Analysis Date = 10/30/15 Pct Recovery = 73% Analysis Date = 10/30/15 Pct Recovery = 73% Analysis Date = 10/21/15 Pct Recovery = 72% Analysis Date = 10/21/15 Pct Recovery = 72% Analysis Date = 10/11/15 Pct Recovery = 72% Analysis Date = 10/11/15 Pct Recovery = 72% Analysis Date = 10/02/15 Pct Recovery = 72% Analysis Date = 10/02/15 Pct Recovery = 72% Analysis Date = 09/23/15 Pct Recovery = 72% Analysis Date = 09/23/15 Pct Recovery = 72% Analysis Date = 09/14/15 Pct Recovery = 72% Analysis Date = 09/14/15 Pct Recovery = 72% Analysis Date = 09/04/15 Pct Recovery = 72% Analysis Date = 09/04/15 Pct Recovery = 72% Analysis Date = 08/26/15 Pct Recovery = 71% Analysis Date = 08/26/15 Pct Recovery = 71% Analysis Date = 08/17/15 Pct Recovery = 71% Analysis Date = 08/17/15 Pct Recovery = 71% Analysis Date = 08/08/15 Pct Recovery = 71% Analysis Date = 08/08/15 Pct Recovery = 71% Analysis Date = 07/30/15 Pct Recovery = 71% Analysis Date = 07/30/15 Pct Recovery = 71% Analysis Date = 07/20/15 Pct Recovery = 71% Analysis Date = 07/20/15 Pct Recovery = 71% Analysis Date = 07/11/15 Pct Recovery = 70% Analysis Date = 07/11/15 Pct Recovery = 70% Analysis Date = 07/02/15 Pct Recovery = 70% Analysis Date = 07/02/15 Pct Recovery = 70% Analysis Date = 06/23/15 Pct Recovery = 70% Analysis Date = 06/23/15 Pct Recovery = 70% Analysis Date = 06/13/15 Pct Recovery = 70% Analysis Date = 06/13/15 Pct Recovery = 70% Analysis Date = 06/04/15 Pct Recovery = 70% Analysis Date = 06/04/15 Pct Recovery = 70% Analysis Date = 05/26/15 Pct Recovery = 70% Analysis Date = 05/26/15 Pct Recovery = 70% Analysis Date = 05/17/15 Pct Recovery = 69% Analysis Date = 05/17/15 Pct Recovery = 69% Analysis Date = 05/07/15 Pct Recovery = 69% Analysis Date = 05/07/15 Pct Recovery = 69% Analysis Date = 04/28/15 Pct Recovery = 69% Analysis Date = 04/28/15 Pct Recovery = 69% Analysis Date = 04/19/15 Pct Recovery = 69% Analysis Date = 04/19/15 Pct Recovery = 69% Analysis Date = 04/10/15 Pct Recovery = 69% Analysis Date = 04/10/15 Pct Recovery = 69% Analysis Date = 03/31/15 Pct Recovery = 69% Analysis Date = 03/31/15 Pct Recovery = 69% Analysis Date = 03/22/15 Pct Recovery = 69% Analysis Date = 03/22/15 Pct Recovery = 69% Analysis Date = 03/13/15 Pct Recovery = 68% Analysis Date = 03/13/15 Pct Recovery = 68% Analysis Date = 03/04/15 Pct Recovery = 68% Analysis Date = 03/04/15 Pct Recovery = 68% Analysis Date = 02/22/15 Pct Recovery = 68% Analysis Date = 02/22/15 Pct Recovery = 68% Analysis Date = 02/13/15 Pct Recovery = 68% Analysis Date = 02/13/15 Pct Recovery = 68% Analysis Date = 02/04/15 Pct Recovery = 68% Analysis Date = 02/04/15 Pct Recovery = 68% Analysis Date = 01/26/15 Pct Recovery = 68% Analysis Date = 01/26/15 Pct Recovery = 68% Analysis Date = 01/16/15 Pct Recovery = 69% Analysis Date = 01/16/15 Pct Recovery = 69% Analysis Date = 01/07/15 Pct Recovery = 69% Analysis Date = 01/07/15 Pct Recovery = 69% Analysis Date = 12/29/14 Pct Recovery = 69% Analysis Date = 12/29/14 Pct Recovery = 69% Analysis Date = 12/20/14 Pct Recovery = 69% Analysis Date = 12/20/14 Pct Recovery = 69% Analysis Date = 12/11/14 Pct Recovery = 69% Analysis Date = 12/11/14 Pct Recovery = 69% Analysis Date = 12/01/14 Pct Recovery = 69% Analysis Date = 12/01/14 Pct Recovery = 69% Analysis Date = 11/22/14 Pct Recovery = 69% Analysis Date = 11/22/14 Pct Recovery = 69% Analysis Date = 11/13/14 Pct Recovery = 70% Analysis Date = 11/13/14 Pct Recovery = 70% Analysis Date = 11/04/14 Pct Recovery = 70% Analysis Date = 11/04/14 Pct Recovery = 70% Analysis Date = 10/25/14 Pct Recovery = 70% Analysis Date = 10/25/14 Pct Recovery = 70% Analysis Date = 10/16/14 Pct Recovery = 70% Analysis Date = 10/16/14 Pct Recovery = 70% Analysis Date = 10/07/14 Pct Recovery = 70% Analysis Date = 10/07/14 Pct Recovery = 70% Analysis Date = 09/28/14 Pct Recovery = 70% Analysis Date = 09/28/14 Pct Recovery = 70% Analysis Date = 09/18/14 Pct Recovery = 70% Analysis Date = 09/18/14 Pct Recovery = 70% Analysis Date = 09/09/14 Pct Recovery = 71% Analysis Date = 09/09/14 Pct Recovery = 71% Analysis Date = 08/31/14 Pct Recovery = 71% Analysis Date = 08/31/14 Pct Recovery = 71% Analysis Date = 08/22/14 Pct Recovery = 71% Analysis Date = 08/22/14 Pct Recovery = 71% Analysis Date = 08/12/14 Pct Recovery = 71% Analysis Date = 08/12/14 Pct Recovery = 71% Analysis Date = 08/03/14 Pct Recovery = 71% Analysis Date = 08/03/14 Pct Recovery = 71% Analysis Date = 07/25/14 Pct Recovery = 71% Analysis Date = 07/25/14 Pct Recovery = 71% Analysis Date = 07/16/14 Pct Recovery = 71% Analysis Date = 07/16/14 Pct Recovery = 71% Analysis Date = 07/06/14 Pct Recovery = 72% Analysis Date = 07/06/14 Pct Recovery = 72% Analysis Date = 06/27/14 Pct Recovery = 72% Analysis Date = 06/27/14 Pct Recovery = 72% Analysis Date = 06/18/14 Pct Recovery = 73% Analysis Date = 06/18/14 Pct Recovery = 73% Analysis Date = 06/09/14 Pct Recovery = 73% Analysis Date = 06/09/14 Pct Recovery = 73% Analysis Date = 05/30/14 Pct Recovery = 74% Analysis Date = 05/30/14 Pct Recovery = 74% Analysis Date = 05/21/14 Pct Recovery = 74% Analysis Date = 05/21/14 Pct Recovery = 74% Analysis Date = 05/12/14 Pct Recovery = 75% Analysis Date = 05/12/14 Pct Recovery = 75% Analysis Date = 05/03/14 Pct Recovery = 75% Analysis Date = 05/03/14 Pct Recovery = 75% Analysis Date = 04/24/14 Pct Recovery = 76% Analysis Date = 04/24/14 Pct Recovery = 76% Analysis Date = 04/14/14 Pct Recovery = 76% Analysis Date = 04/14/14 Pct Recovery = 76% Analysis Date = 04/05/14 Pct Recovery = 77% Analysis Date = 04/05/14 Pct Recovery = 77% Analysis Date = 03/27/14 Pct Recovery = 77% Analysis Date = 03/27/14 Pct Recovery = 77% Analysis Date = 03/18/14 Pct Recovery = 78% Analysis Date = 03/18/14 Pct Recovery = 78% Analysis Date = 03/08/14 Pct Recovery = 78% Analysis Date = 03/08/14 Pct Recovery = 78% Analysis Date = 02/27/14 Pct Recovery = 79% Analysis Date = 02/27/14 Pct Recovery = 79% Analysis Date = 02/18/14 Pct Recovery = 79% Analysis Date = 02/18/14 Pct Recovery = 79% Analysis Date = 02/09/14 Pct Recovery = 80% Analysis Date = 02/09/14 Pct Recovery = 80% Analysis Date = 01/30/14 Pct Recovery = 80% Analysis Date = 01/30/14 Pct Recovery = 80% Analysis Date = 01/21/14 Pct Recovery = 81% Analysis Date = 01/21/14 Pct Recovery = 81% Analysis Date = 01/12/14 Pct Recovery = 81% Analysis Date = 01/12/14 Pct Recovery = 81% Analysis Date = 01/03/14 Pct Recovery = 82% Analysis Date = 01/03/14 Pct Recovery = 82% Analysis Date = 12/24/13 Pct Recovery = 82% Analysis Date = 12/24/13 Pct Recovery = 82% Analysis Date = 12/15/13 Pct Recovery = 83% Analysis Date = 12/15/13 Pct Recovery = 83% Analysis Date = 12/06/13 Pct Recovery = 83% Analysis Date = 12/06/13 Pct Recovery = 83% Analysis Date = 11/27/13 Pct Recovery = 84% Analysis Date = 11/27/13 Pct Recovery = 84% Analysis Date = 11/17/13 Pct Recovery = 84% Analysis Date = 11/17/13 Pct Recovery = 84% Analysis Date = 11/08/13 Pct Recovery = 85% Analysis Date = 11/08/13 Pct Recovery = 85% Analysis Date = 10/30/13 Pct Recovery = 85% Analysis Date = 10/30/13 Pct Recovery = 85% Analysis Date = 10/21/13 Pct Recovery = 85% Analysis Date = 10/21/13 Pct Recovery = 85% Analysis Date = 10/11/13 Pct Recovery = 86% Analysis Date = 10/11/13 Pct Recovery = 86% Analysis Date = 10/02/13 Pct Recovery = 86% Analysis Date = 10/02/13 Pct Recovery = 86% Analysis Date = 09/23/13 Pct Recovery = 87% Analysis Date = 09/23/13 Pct Recovery = 87% Analysis Date = 09/14/13 Pct Recovery = 87% Analysis Date = 09/14/13 Pct Recovery = 87% Analysis Date = 09/05/13 Pct Recovery = 88% Analysis Date = 09/05/13 Pct Recovery = 88% Analysis Date = 08/26/13 Pct Recovery = 88% Analysis Date = 08/26/13 Pct Recovery = 88% Analysis Date = 08/17/13 Pct Recovery = 89% Analysis Date = 08/17/13 Pct Recovery = 89% Analysis Date = 08/08/13 Pct Recovery = 89% Analysis Date = 08/08/13 Pct Recovery = 89% Analysis Date = 07/30/13 Pct Recovery = 90% Analysis Date = 07/30/13 Pct Recovery = 90% Analysis Date = 07/20/13 Pct Recovery = 90% Analysis Date = 07/20/13 Pct Recovery = 90% Analysis Date = 07/11/13 Pct Recovery = 90% Analysis Date = 07/11/13 Pct Recovery = 90% Analysis Date = 07/02/13 Pct Recovery = 91% Analysis Date = 07/02/13 Pct Recovery = 91% Analysis Date = 06/23/13 Pct Recovery = 91% Analysis Date = 06/23/13 Pct Recovery = 91% Analysis Date = 06/13/13 Pct Recovery = 92% Analysis Date = 06/13/13 Pct Recovery = 92% Analysis Date = 06/04/13 Pct Recovery = 92% Analysis Date = 06/04/13 Pct Recovery = 92% Analysis Date = 05/26/13 Pct Recovery = 93% Analysis Date = 05/26/13 Pct Recovery = 93% Analysis Date = 05/17/13 Pct Recovery = 93% Analysis Date = 05/17/13 Pct Recovery = 93% Analysis Date = 05/07/13 Pct Recovery = 94% Analysis Date = 05/07/13 Pct Recovery = 94% Analysis Date = 04/28/13 Pct Recovery = 94% Analysis Date = 04/28/13 Pct Recovery = 94% Analysis Date = 04/19/13 Pct Recovery = 95% Analysis Date = 04/19/13 Pct Recovery = 95% Analysis Date = 04/10/13 Pct Recovery = 95% Analysis Date = 04/10/13 Pct Recovery = 95% Analysis Date = 03/31/13 Pct Recovery = 95% Analysis Date = 03/31/13 Pct Recovery = 95% Analysis Date = 03/22/13 Pct Recovery = 96% Analysis Date = 03/22/13 Pct Recovery = 96% Analysis Date = 03/13/13 Pct Recovery = 96% Analysis Date = 03/13/13 Pct Recovery = 96% Analysis Date = 03/04/13 Pct Recovery = 97% Analysis Date = 03/04/13 Pct Recovery = 97% Analysis Date = 02/22/13 Pct Recovery = 97% Analysis Date = 02/22/13 Pct Recovery = 97% Analysis Date = 02/13/13 Pct Recovery = 98% Analysis Date = 02/13/13 Pct Recovery = 98% Analysis Date = 02/04/13 Pct Recovery = 98% Analysis Date = 02/04/13 Pct Recovery = 98% Analysis Date = 01/26/13 Pct Recovery = 98% Analysis Date = 01/26/13 Pct Recovery = 98% Analysis Date = 01/17/13 Pct Recovery = 99% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
FENAMIPHOS SULFONE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 76 77% 22% 75% 18%
Total 76 77% 22% 75% 18%

Sample Statistics
FENAMIPHOS SULFONE

Characteristic N % % Basis
Plotted 76 100% Spiked
Estimated Values 7 9% Spiked
Deleted Values 1 1% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 76 .  
False Negatives 0 0% 0 out of 76
Not Spiked 42 .  
False Positives 3 7% 3 out of 41

OBSP Determination:
FENAMIPHOS SULFOXIDE
METHOD: 2033 , TESTIDCODE: 61646GCM39

Laboratory ID = 20140100085 Lab Value = 0.134 Expected Conc. = 0.811 Report level label = 0.08 Pct Recovery = 17% Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl SpecificMix = 042413 Laboratory ID = 20172510330 Lab Value = 0.108 Expected Conc. = 0.535 Report level label = 0.08 Pct Recovery = 20% Analysis Date = 12/29/17 SpikeMix = ChemService 6537100: 100 µl & Abs 071817Pest: 100 µl SpecificMix = 071817Pest Laboratory ID = 20163370001 Lab Value = 0.100 Expected Conc. = 0.5 Report level label = 0.08 Pct Recovery = 20% Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl SpecificMix = B20160331 Laboratory ID = 20163150006 Lab Value = 0.087 Expected Conc. = 0.5 Report level label = 0.08 Pct Recovery = 17% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl SpecificMix = B20160331 Laboratory ID = 20161880109 Lab Value = 0.078 Expected Conc. = 0.497 Report level label = 0.08 Pct Recovery = 16% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl SpecificMix = 03FF076 Laboratory ID = 20130250061 Lab Value = 0.171 Expected Conc. = 0.493 Report level label = 0.08 Pct Recovery = 35% Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl SpecificMix = 05BB029 Laboratory ID = 20152750006 Lab Value = 0.059 Expected Conc. = 0.48 Report level label = 0.08 Pct Recovery = 12% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl SpecificMix = EN150514012 Laboratory ID = 20132690010 Lab Value = 0.102 Expected Conc. = 0.4055 Report level label = 0.08 Pct Recovery = 25% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl SpecificMix = 042413 Laboratory ID = 20132560001 Lab Value = 0.092 Expected Conc. = 0.4055 Report level label = 0.08 Pct Recovery = 23% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl SpecificMix = 042413 Laboratory ID = 20171720140 Lab Value = 0.048 Expected Conc. = 0.4 Report level label = 0.08 Pct Recovery = 12% Analysis Date = 08/31/17 SpikeMix = Supelco LC20138V: 80 µl & Phenova B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20171660002 Lab Value = 0.053 Expected Conc. = 0.4 Report level label = 0.08 Pct Recovery = 13% Analysis Date = 08/23/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20170190026 Lab Value = 0.063 Expected Conc. = 0.4 Report level label = 0.08 Pct Recovery = 16% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20161470001 Lab Value = 0.059 Expected Conc. = 0.4 Report level label = 0.08 Pct Recovery = 15% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20170960001 Lab Value = 0.069 Expected Conc. = 0.3976 Report level label = 0.08 Pct Recovery = 17% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl SpecificMix = 03FF076 Laboratory ID = 20132140002 Lab Value = 0.118 Expected Conc. = 0.394 Report level label = 0.08 Pct Recovery = 30% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl SpecificMix = 04CC101 Laboratory ID = 20150720069 Lab Value = 0.079 Expected Conc. = 0.321 Report level label = 0.08 Pct Recovery = 25% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 0227-14-08 Laboratory ID = 20141770149 Lab Value = 0.078 Expected Conc. = 0.321 Report level label = 0.08 Pct Recovery = 24% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl SpecificMix = 0227-14-08 Laboratory ID = 20141570088 Lab Value = 0.043 Expected Conc. = 0.321 Report level label = 0.08 Pct Recovery = 13% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl SpecificMix = 0227-14-08 Laboratory ID = 20150430092 Lab Value = 0.054 Expected Conc. = 0.3204 Report level label = 0.08 Pct Recovery = 17% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl SpecificMix = 042814 Laboratory ID = 20143240095 Lab Value = 0.044 Expected Conc. = 0.3204 Report level label = 0.08 Pct Recovery = 14% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl SpecificMix = 042814 Laboratory ID = 20142960086 Lab Value = 0.050 Expected Conc. = 0.3204 Report level label = 0.08 Pct Recovery = 16% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 042814 Laboratory ID = 20142530087 Lab Value = 0.028 Expected Conc. = 0.3204 Report level label = 0.08 Pct Recovery = 9% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl SpecificMix = 042814 Laboratory ID = 20173480003 Lab Value = 0.033 Expected Conc. = 0.27 Report level label = 0.14 Pct Recovery = 12% Analysis Date = 04/05/18 SpikeMix = Abs 071717Pest: 50 µl & ChemService 6567600: 50 µl SpecificMix = 6567600 Laboratory ID = 20172560101 Lab Value = 0.053 Expected Conc. = 0.27 Report level label = 0.08 Pct Recovery = 20% Analysis Date = 12/22/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6567600: 50 µl SpecificMix = 6567600 Laboratory ID = 20181430122 Lab Value = 0.040 Expected Conc. = 0.2675 Report level label = 0.14 Pct Recovery = 15% Analysis Date = 06/20/18 SpikeMix = Abs 071817Pest: 50 µl & Spex Organics EN170808006: 50 µl SpecificMix = 071817Pest Laboratory ID = 20140230082 Lab Value = 0.068 Expected Conc. = 0.2505 Report level label = 0.08 Pct Recovery = 27% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl SpecificMix = 012513 Laboratory ID = 20132420001 Lab Value = 0.109 Expected Conc. = 0.2505 Report level label = 0.08 Pct Recovery = 44% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl SpecificMix = 012513 Laboratory ID = 20130940097 Lab Value = 0.198 Expected Conc. = 0.2505 Report level label = 0.08 Pct Recovery = 79% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = 052412 Laboratory ID = 20130100066 Lab Value = 0.118 Expected Conc. = 0.2505 Report level label = 0.08 Pct Recovery = 47% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl SpecificMix = 052412 Laboratory ID = 20152330039 Lab Value = 0.032 Expected Conc. = 0.242 Report level label = 0.08 Pct Recovery = 13% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl SpecificMix = 041415 Laboratory ID = 20151900132 Lab Value = 0.039 Expected Conc. = 0.242 Report level label = 0.08 Pct Recovery = 16% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl SpecificMix = 041415 Laboratory ID = 20151270112 Lab Value = 0.040 Expected Conc. = 0.242 Report level label = 0.08 Pct Recovery = 17% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl SpecificMix = 041415 Laboratory ID = 20160630046 Lab Value = 0.037 Expected Conc. = 0.24 Report level label = 0.08 Pct Recovery = 15% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = EN150514012 Laboratory ID = 20153440001 Lab Value = 0.017 Expected Conc. = 0.24 Report level label = 0.08 Pct Recovery = 7% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = EN150514012 Laboratory ID = 20171160110 Lab Value = 0.064 Expected Conc. = 0.2 Report level label = 0.08 Pct Recovery = 32% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = B20160331 Laboratory ID = 20162380004 Lab Value = 0.025 Expected Conc. = 0.2 Report level label = 0.08 Pct Recovery = 13% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = B20160331 Laboratory ID = 20172020035 Lab Value = 0.027 Expected Conc. = 0.1988 Report level label = 0.08 Pct Recovery = 14% Analysis Date = 11/07/17 SpikeMix = Abs 071717Pest: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20171510080 Lab Value = 0.051 Expected Conc. = 0.1988 Report level label = 0.08 Pct Recovery = 26% Analysis Date = 06/09/17 SpikeMix = Supelco LC20138V: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20170460061 Lab Value = 0.035 Expected Conc. = 0.1988 Report level label = 0.08 Pct Recovery = 18% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl SpecificMix = 03FF076 Laboratory ID = 20162660005 Lab Value = 0.045 Expected Conc. = 0.1988 Report level label = 0.08 Pct Recovery = 23% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl SpecificMix = 03FF076 Laboratory ID = 20161600087 Lab Value = 0.016 Expected Conc. = 0.1988 Report level label = 0.08 Pct Recovery = 8% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20133580036 Lab Value = 0.035 Expected Conc. = 0.1622 Report level label = 0.08 Pct Recovery = 22% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 042413 Laboratory ID = 20133190012 Lab Value = 0.042 Expected Conc. = 0.1622 Report level label = 0.08 Pct Recovery = 26% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 042413 Laboratory ID = 20131650073 Lab Value = 0.096 Expected Conc. = 0.1622 Report level label = 0.08 Pct Recovery = 59% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl SpecificMix = 042413 Laboratory ID = 20180730064 Lab Value = 0.040 Expected Conc. = 0.1605 Report level label = 0.14 Pct Recovery = 25% Analysis Date = 05/16/18 SpikeMix = Abs 071717Pest: 30 µl & Abs 071817Pest: 30 µl SpecificMix = 071817Pest Laboratory ID = 20180050004 Lab Value = 0.033 Expected Conc. = 0.1605 Report level label = 0.14 Pct Recovery = 21% Analysis Date = 04/05/18 SpikeMix = Abs 071817Pest: 30 µl & ChemService 6472100: 30 µl SpecificMix = 071817Pest Laboratory ID = 20172780018 Lab Value = 0.038 Expected Conc. = 0.1605 Report level label = 0.08 Pct Recovery = 24% Analysis Date = 02/08/18 SpikeMix = ChemService 6537100: 30 µl & Abs 071817Pest: 30 µl SpecificMix = 071817Pest Laboratory ID = 20141490205 Lab Value = 0.024 Expected Conc. = 0.1605 Report level label = 0.08 Pct Recovery = 15% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20141420140 Lab Value = 0.040 Expected Conc. = 0.1605 Report level label = 0.08 Pct Recovery = 25% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20143370094 Lab Value = 0.021 Expected Conc. = 0.1602 Report level label = 0.08 Pct Recovery = 13% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl SpecificMix = 042814 Laboratory ID = 20142820151 Lab Value = 0.071 Expected Conc. = 0.1602 Report level label = 0.08 Pct Recovery = 44% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl SpecificMix = 042814 Laboratory ID = 20142470041 Lab Value = 0.040 Expected Conc. = 0.1602 Report level label = 0.08 Pct Recovery = 25% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl SpecificMix = 042814 Laboratory ID = 20142200164 Lab Value = 0.033 Expected Conc. = 0.1602 Report level label = 0.08 Pct Recovery = 21% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 042814 Laboratory ID = 20140730138 Lab Value = 0.050 Expected Conc. = 0.1576 Report level label = 0.08 Pct Recovery = 32% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 04CC101 Laboratory ID = 20140510043 Lab Value = 0.153 Expected Conc. = 0.1576 Report level label = 0.08 Pct Recovery = 97% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 04CC101 Laboratory ID = 20133310030 Lab Value = 0.036 Expected Conc. = 0.1576 Report level label = 0.08 Pct Recovery = 23% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl SpecificMix = 04CC101 Laboratory ID = 20132280016 Lab Value = 0.094 Expected Conc. = 0.1576 Report level label = 0.08 Pct Recovery = 60% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl SpecificMix = 04CC101 Laboratory ID = 20131510026 Lab Value = 0.123 Expected Conc. = 0.1576 Report level label = 0.08 Pct Recovery = 78% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl SpecificMix = 04CC101 Laboratory ID = 20161050143 Lab Value = 0.015 Expected Conc. = 0.121 Report level label = 0.08 Pct Recovery = 12% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 041415 Laboratory ID = 20160560044 Lab Value = 0.007 Expected Conc. = 0.121 Report level label = 0.08 Pct Recovery = 6% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl SpecificMix = 041415 Laboratory ID = 20152950078 Lab Value = 0.018 Expected Conc. = 0.121 Report level label = 0.08 Pct Recovery = 15% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 041415 Laboratory ID = 20152040177 Lab Value = 0.030 Expected Conc. = 0.121 Report level label = 0.08 Pct Recovery = 25% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl SpecificMix = 041415 Laboratory ID = 20151210037 Lab Value = 0.018 Expected Conc. = 0.121 Report level label = 0.08 Pct Recovery = 15% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 041415 Laboratory ID = 20160070059 Lab Value = 0.012 Expected Conc. = 0.12 Report level label = 0.08 Pct Recovery = 10% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = EN150514012 Laboratory ID = 20151760208 Lab Value = 0.044 Expected Conc. = 0.12 Report level label = 0.08 Pct Recovery = 37% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl SpecificMix = EN150514012 Laboratory ID = 20151480170 Lab Value = 0.021 Expected Conc. = 0.12 Report level label = 0.08 Pct Recovery = 18% Analysis Date = 06/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150514012 Laboratory ID = 20140860102 Lab Value = 0.024 Expected Conc. = 0.1002 Report level label = 0.08 Pct Recovery = 24% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 012513 Laboratory ID = 20133400002 Lab Value = 0.035 Expected Conc. = 0.1002 Report level label = 0.08 Pct Recovery = 35% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = 052412 Laboratory ID = 20131920149 Lab Value = 0.064 Expected Conc. = 0.1002 Report level label = 0.08 Pct Recovery = 64% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl SpecificMix = 012513 Laboratory ID = 20130650005 Lab Value = 0.048 Expected Conc. = 0.1002 Report level label = 0.08 Pct Recovery = 48% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl SpecificMix = 052412 Laboratory ID = 20131230084 Lab Value = 0.122 Expected Conc. = 0.0986 Report level label = 0.08 Pct Recovery = 124% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl SpecificMix = 05BB029 Laboratory ID = 20130510051 Lab Value = 0.072 Expected Conc. = 0.0986 Report level label = 0.08 Pct Recovery = 73% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl SpecificMix = 05BB029 Analysis Date = 06/20/18 Pct Recovery = 20% Analysis Date = 06/10/18 Pct Recovery = 20% Analysis Date = 06/10/18 Pct Recovery = 20% Analysis Date = 05/31/18 Pct Recovery = 20% Analysis Date = 05/31/18 Pct Recovery = 20% Analysis Date = 05/21/18 Pct Recovery = 20% Analysis Date = 05/21/18 Pct Recovery = 20% Analysis Date = 05/11/18 Pct Recovery = 20% Analysis Date = 05/11/18 Pct Recovery = 20% Analysis Date = 05/01/18 Pct Recovery = 19% Analysis Date = 05/01/18 Pct Recovery = 19% Analysis Date = 04/21/18 Pct Recovery = 19% Analysis Date = 04/21/18 Pct Recovery = 19% Analysis Date = 04/11/18 Pct Recovery = 19% Analysis Date = 04/11/18 Pct Recovery = 19% Analysis Date = 04/01/18 Pct Recovery = 19% Analysis Date = 04/01/18 Pct Recovery = 19% Analysis Date = 03/22/18 Pct Recovery = 19% Analysis Date = 03/22/18 Pct Recovery = 19% Analysis Date = 03/13/18 Pct Recovery = 19% Analysis Date = 03/13/18 Pct Recovery = 19% Analysis Date = 03/03/18 Pct Recovery = 19% Analysis Date = 03/03/18 Pct Recovery = 19% Analysis Date = 02/21/18 Pct Recovery = 19% Analysis Date = 02/21/18 Pct Recovery = 19% Analysis Date = 02/11/18 Pct Recovery = 19% Analysis Date = 02/11/18 Pct Recovery = 19% Analysis Date = 02/01/18 Pct Recovery = 19% Analysis Date = 02/01/18 Pct Recovery = 19% Analysis Date = 01/22/18 Pct Recovery = 19% Analysis Date = 01/22/18 Pct Recovery = 19% Analysis Date = 01/12/18 Pct Recovery = 19% Analysis Date = 01/12/18 Pct Recovery = 19% Analysis Date = 01/02/18 Pct Recovery = 19% Analysis Date = 01/02/18 Pct Recovery = 19% Analysis Date = 12/23/17 Pct Recovery = 19% Analysis Date = 12/23/17 Pct Recovery = 19% Analysis Date = 12/13/17 Pct Recovery = 19% Analysis Date = 12/13/17 Pct Recovery = 19% Analysis Date = 12/04/17 Pct Recovery = 19% Analysis Date = 12/04/17 Pct Recovery = 19% Analysis Date = 11/24/17 Pct Recovery = 18% Analysis Date = 11/24/17 Pct Recovery = 18% Analysis Date = 11/14/17 Pct Recovery = 18% Analysis Date = 11/14/17 Pct Recovery = 18% Analysis Date = 11/04/17 Pct Recovery = 18% Analysis Date = 11/04/17 Pct Recovery = 18% Analysis Date = 10/25/17 Pct Recovery = 18% Analysis Date = 10/25/17 Pct Recovery = 18% Analysis Date = 10/15/17 Pct Recovery = 18% Analysis Date = 10/15/17 Pct Recovery = 18% Analysis Date = 10/05/17 Pct Recovery = 18% Analysis Date = 10/05/17 Pct Recovery = 18% Analysis Date = 09/25/17 Pct Recovery = 18% Analysis Date = 09/25/17 Pct Recovery = 18% Analysis Date = 09/15/17 Pct Recovery = 18% Analysis Date = 09/15/17 Pct Recovery = 18% Analysis Date = 09/05/17 Pct Recovery = 18% Analysis Date = 09/05/17 Pct Recovery = 18% Analysis Date = 08/27/17 Pct Recovery = 18% Analysis Date = 08/27/17 Pct Recovery = 18% Analysis Date = 08/17/17 Pct Recovery = 18% Analysis Date = 08/17/17 Pct Recovery = 18% Analysis Date = 08/07/17 Pct Recovery = 18% Analysis Date = 08/07/17 Pct Recovery = 18% Analysis Date = 07/28/17 Pct Recovery = 18% Analysis Date = 07/28/17 Pct Recovery = 18% Analysis Date = 07/18/17 Pct Recovery = 18% Analysis Date = 07/18/17 Pct Recovery = 18% Analysis Date = 07/08/17 Pct Recovery = 18% Analysis Date = 07/08/17 Pct Recovery = 18% Analysis Date = 06/28/17 Pct Recovery = 18% Analysis Date = 06/28/17 Pct Recovery = 18% Analysis Date = 06/18/17 Pct Recovery = 18% Analysis Date = 06/18/17 Pct Recovery = 18% Analysis Date = 06/08/17 Pct Recovery = 18% Analysis Date = 06/08/17 Pct Recovery = 18% Analysis Date = 05/29/17 Pct Recovery = 17% Analysis Date = 05/29/17 Pct Recovery = 17% Analysis Date = 05/20/17 Pct Recovery = 17% Analysis Date = 05/20/17 Pct Recovery = 17% Analysis Date = 05/10/17 Pct Recovery = 17% Analysis Date = 05/10/17 Pct Recovery = 17% Analysis Date = 04/30/17 Pct Recovery = 17% Analysis Date = 04/30/17 Pct Recovery = 17% Analysis Date = 04/20/17 Pct Recovery = 17% Analysis Date = 04/20/17 Pct Recovery = 17% Analysis Date = 04/10/17 Pct Recovery = 17% Analysis Date = 04/10/17 Pct Recovery = 17% Analysis Date = 03/31/17 Pct Recovery = 17% Analysis Date = 03/31/17 Pct Recovery = 17% Analysis Date = 03/21/17 Pct Recovery = 17% Analysis Date = 03/21/17 Pct Recovery = 17% Analysis Date = 03/11/17 Pct Recovery = 17% Analysis Date = 03/11/17 Pct Recovery = 17% Analysis Date = 03/01/17 Pct Recovery = 17% Analysis Date = 03/01/17 Pct Recovery = 17% Analysis Date = 02/19/17 Pct Recovery = 17% Analysis Date = 02/19/17 Pct Recovery = 17% Analysis Date = 02/10/17 Pct Recovery = 17% Analysis Date = 02/10/17 Pct Recovery = 17% Analysis Date = 01/31/17 Pct Recovery = 17% Analysis Date = 01/31/17 Pct Recovery = 17% Analysis Date = 01/21/17 Pct Recovery = 17% Analysis Date = 01/21/17 Pct Recovery = 17% Analysis Date = 01/11/17 Pct Recovery = 17% Analysis Date = 01/11/17 Pct Recovery = 17% Analysis Date = 01/01/17 Pct Recovery = 17% Analysis Date = 01/01/17 Pct Recovery = 17% Analysis Date = 12/22/16 Pct Recovery = 17% Analysis Date = 12/22/16 Pct Recovery = 17% Analysis Date = 12/12/16 Pct Recovery = 17% Analysis Date = 12/12/16 Pct Recovery = 17% Analysis Date = 12/02/16 Pct Recovery = 17% Analysis Date = 12/02/16 Pct Recovery = 17% Analysis Date = 11/22/16 Pct Recovery = 17% Analysis Date = 11/22/16 Pct Recovery = 17% Analysis Date = 11/12/16 Pct Recovery = 17% Analysis Date = 11/12/16 Pct Recovery = 17% Analysis Date = 11/03/16 Pct Recovery = 17% Analysis Date = 11/03/16 Pct Recovery = 17% Analysis Date = 10/24/16 Pct Recovery = 17% Analysis Date = 10/24/16 Pct Recovery = 17% Analysis Date = 10/14/16 Pct Recovery = 17% Analysis Date = 10/14/16 Pct Recovery = 17% Analysis Date = 10/04/16 Pct Recovery = 17% Analysis Date = 10/04/16 Pct Recovery = 17% Analysis Date = 09/24/16 Pct Recovery = 16% Analysis Date = 09/24/16 Pct Recovery = 16% Analysis Date = 09/14/16 Pct Recovery = 16% Analysis Date = 09/14/16 Pct Recovery = 16% Analysis Date = 09/04/16 Pct Recovery = 16% Analysis Date = 09/04/16 Pct Recovery = 16% Analysis Date = 08/25/16 Pct Recovery = 16% Analysis Date = 08/25/16 Pct Recovery = 16% Analysis Date = 08/15/16 Pct Recovery = 16% Analysis Date = 08/15/16 Pct Recovery = 16% Analysis Date = 08/05/16 Pct Recovery = 16% Analysis Date = 08/05/16 Pct Recovery = 16% Analysis Date = 07/27/16 Pct Recovery = 16% Analysis Date = 07/27/16 Pct Recovery = 16% Analysis Date = 07/17/16 Pct Recovery = 16% Analysis Date = 07/17/16 Pct Recovery = 16% Analysis Date = 07/07/16 Pct Recovery = 16% Analysis Date = 07/07/16 Pct Recovery = 16% Analysis Date = 06/27/16 Pct Recovery = 16% Analysis Date = 06/27/16 Pct Recovery = 16% Analysis Date = 06/17/16 Pct Recovery = 16% Analysis Date = 06/17/16 Pct Recovery = 16% Analysis Date = 06/07/16 Pct Recovery = 16% Analysis Date = 06/07/16 Pct Recovery = 16% Analysis Date = 05/28/16 Pct Recovery = 16% Analysis Date = 05/28/16 Pct Recovery = 16% Analysis Date = 05/18/16 Pct Recovery = 16% Analysis Date = 05/18/16 Pct Recovery = 16% Analysis Date = 05/08/16 Pct Recovery = 16% Analysis Date = 05/08/16 Pct Recovery = 16% Analysis Date = 04/28/16 Pct Recovery = 16% Analysis Date = 04/28/16 Pct Recovery = 16% Analysis Date = 04/19/16 Pct Recovery = 16% Analysis Date = 04/19/16 Pct Recovery = 16% Analysis Date = 04/09/16 Pct Recovery = 16% Analysis Date = 04/09/16 Pct Recovery = 16% Analysis Date = 03/30/16 Pct Recovery = 16% Analysis Date = 03/30/16 Pct Recovery = 16% Analysis Date = 03/20/16 Pct Recovery = 16% Analysis Date = 03/20/16 Pct Recovery = 16% Analysis Date = 03/10/16 Pct Recovery = 16% Analysis Date = 03/10/16 Pct Recovery = 16% Analysis Date = 02/29/16 Pct Recovery = 16% Analysis Date = 02/29/16 Pct Recovery = 16% Analysis Date = 02/19/16 Pct Recovery = 16% Analysis Date = 02/19/16 Pct Recovery = 16% Analysis Date = 02/09/16 Pct Recovery = 16% Analysis Date = 02/09/16 Pct Recovery = 16% Analysis Date = 01/30/16 Pct Recovery = 16% Analysis Date = 01/30/16 Pct Recovery = 16% Analysis Date = 01/20/16 Pct Recovery = 16% Analysis Date = 01/20/16 Pct Recovery = 16% Analysis Date = 01/11/16 Pct Recovery = 16% Analysis Date = 01/11/16 Pct Recovery = 16% Analysis Date = 01/01/16 Pct Recovery = 16% Analysis Date = 01/01/16 Pct Recovery = 16% Analysis Date = 12/22/15 Pct Recovery = 16% Analysis Date = 12/22/15 Pct Recovery = 16% Analysis Date = 12/12/15 Pct Recovery = 16% Analysis Date = 12/12/15 Pct Recovery = 16% Analysis Date = 12/02/15 Pct Recovery = 16% Analysis Date = 12/02/15 Pct Recovery = 16% Analysis Date = 11/22/15 Pct Recovery = 17% Analysis Date = 11/22/15 Pct Recovery = 17% Analysis Date = 11/12/15 Pct Recovery = 17% Analysis Date = 11/12/15 Pct Recovery = 17% Analysis Date = 11/02/15 Pct Recovery = 17% Analysis Date = 11/02/15 Pct Recovery = 17% Analysis Date = 10/23/15 Pct Recovery = 17% Analysis Date = 10/23/15 Pct Recovery = 17% Analysis Date = 10/13/15 Pct Recovery = 17% Analysis Date = 10/13/15 Pct Recovery = 17% Analysis Date = 10/04/15 Pct Recovery = 17% Analysis Date = 10/04/15 Pct Recovery = 17% Analysis Date = 09/24/15 Pct Recovery = 17% Analysis Date = 09/24/15 Pct Recovery = 17% Analysis Date = 09/14/15 Pct Recovery = 17% Analysis Date = 09/14/15 Pct Recovery = 17% Analysis Date = 09/04/15 Pct Recovery = 17% Analysis Date = 09/04/15 Pct Recovery = 17% Analysis Date = 08/25/15 Pct Recovery = 17% Analysis Date = 08/25/15 Pct Recovery = 17% Analysis Date = 08/15/15 Pct Recovery = 17% Analysis Date = 08/15/15 Pct Recovery = 17% Analysis Date = 08/05/15 Pct Recovery = 17% Analysis Date = 08/05/15 Pct Recovery = 17% Analysis Date = 07/26/15 Pct Recovery = 17% Analysis Date = 07/26/15 Pct Recovery = 17% Analysis Date = 07/16/15 Pct Recovery = 17% Analysis Date = 07/16/15 Pct Recovery = 17% Analysis Date = 07/06/15 Pct Recovery = 17% Analysis Date = 07/06/15 Pct Recovery = 17% Analysis Date = 06/27/15 Pct Recovery = 18% Analysis Date = 06/27/15 Pct Recovery = 18% Analysis Date = 06/17/15 Pct Recovery = 18% Analysis Date = 06/17/15 Pct Recovery = 18% Analysis Date = 06/07/15 Pct Recovery = 18% Analysis Date = 06/07/15 Pct Recovery = 18% Analysis Date = 05/28/15 Pct Recovery = 18% Analysis Date = 05/28/15 Pct Recovery = 18% Analysis Date = 05/18/15 Pct Recovery = 18% Analysis Date = 05/18/15 Pct Recovery = 18% Analysis Date = 05/08/15 Pct Recovery = 19% Analysis Date = 05/08/15 Pct Recovery = 19% Analysis Date = 04/28/15 Pct Recovery = 19% Analysis Date = 04/28/15 Pct Recovery = 19% Analysis Date = 04/18/15 Pct Recovery = 19% Analysis Date = 04/18/15 Pct Recovery = 19% Analysis Date = 04/08/15 Pct Recovery = 19% Analysis Date = 04/08/15 Pct Recovery = 19% Analysis Date = 03/29/15 Pct Recovery = 19% Analysis Date = 03/29/15 Pct Recovery = 19% Analysis Date = 03/20/15 Pct Recovery = 20% Analysis Date = 03/20/15 Pct Recovery = 20% Analysis Date = 03/10/15 Pct Recovery = 20% Analysis Date = 03/10/15 Pct Recovery = 20% Analysis Date = 02/28/15 Pct Recovery = 20% Analysis Date = 02/28/15 Pct Recovery = 20% Analysis Date = 02/18/15 Pct Recovery = 20% Analysis Date = 02/18/15 Pct Recovery = 20% Analysis Date = 02/08/15 Pct Recovery = 21% Analysis Date = 02/08/15 Pct Recovery = 21% Analysis Date = 01/29/15 Pct Recovery = 21% Analysis Date = 01/29/15 Pct Recovery = 21% Analysis Date = 01/19/15 Pct Recovery = 21% Analysis Date = 01/19/15 Pct Recovery = 21% Analysis Date = 01/09/15 Pct Recovery = 21% Analysis Date = 01/09/15 Pct Recovery = 21% Analysis Date = 12/30/14 Pct Recovery = 22% Analysis Date = 12/30/14 Pct Recovery = 22% Analysis Date = 12/20/14 Pct Recovery = 22% Analysis Date = 12/20/14 Pct Recovery = 22% Analysis Date = 12/11/14 Pct Recovery = 22% Analysis Date = 12/11/14 Pct Recovery = 22% Analysis Date = 12/01/14 Pct Recovery = 22% Analysis Date = 12/01/14 Pct Recovery = 22% Analysis Date = 11/21/14 Pct Recovery = 23% Analysis Date = 11/21/14 Pct Recovery = 23% Analysis Date = 11/11/14 Pct Recovery = 23% Analysis Date = 11/11/14 Pct Recovery = 23% Analysis Date = 11/01/14 Pct Recovery = 23% Analysis Date = 11/01/14 Pct Recovery = 23% Analysis Date = 10/22/14 Pct Recovery = 23% Analysis Date = 10/22/14 Pct Recovery = 23% Analysis Date = 10/12/14 Pct Recovery = 24% Analysis Date = 10/12/14 Pct Recovery = 24% Analysis Date = 10/02/14 Pct Recovery = 24% Analysis Date = 10/02/14 Pct Recovery = 24% Analysis Date = 09/22/14 Pct Recovery = 24% Analysis Date = 09/22/14 Pct Recovery = 24% Analysis Date = 09/12/14 Pct Recovery = 25% Analysis Date = 09/12/14 Pct Recovery = 25% Analysis Date = 09/03/14 Pct Recovery = 25% Analysis Date = 09/03/14 Pct Recovery = 25% Analysis Date = 08/24/14 Pct Recovery = 25% Analysis Date = 08/24/14 Pct Recovery = 25% Analysis Date = 08/14/14 Pct Recovery = 26% Analysis Date = 08/14/14 Pct Recovery = 26% Analysis Date = 08/04/14 Pct Recovery = 26% Analysis Date = 08/04/14 Pct Recovery = 26% Analysis Date = 07/25/14 Pct Recovery = 26% Analysis Date = 07/25/14 Pct Recovery = 26% Analysis Date = 07/15/14 Pct Recovery = 27% Analysis Date = 07/15/14 Pct Recovery = 27% Analysis Date = 07/05/14 Pct Recovery = 27% Analysis Date = 07/05/14 Pct Recovery = 27% Analysis Date = 06/25/14 Pct Recovery = 28% Analysis Date = 06/25/14 Pct Recovery = 28% Analysis Date = 06/15/14 Pct Recovery = 28% Analysis Date = 06/15/14 Pct Recovery = 28% Analysis Date = 06/05/14 Pct Recovery = 29% Analysis Date = 06/05/14 Pct Recovery = 29% Analysis Date = 05/27/14 Pct Recovery = 29% Analysis Date = 05/27/14 Pct Recovery = 29% Analysis Date = 05/17/14 Pct Recovery = 30% Analysis Date = 05/17/14 Pct Recovery = 30% Analysis Date = 05/07/14 Pct Recovery = 30% Analysis Date = 05/07/14 Pct Recovery = 30% Analysis Date = 04/27/14 Pct Recovery = 30% Analysis Date = 04/27/14 Pct Recovery = 30% Analysis Date = 04/17/14 Pct Recovery = 31% Analysis Date = 04/17/14 Pct Recovery = 31% Analysis Date = 04/07/14 Pct Recovery = 32% Analysis Date = 04/07/14 Pct Recovery = 32% Analysis Date = 03/28/14 Pct Recovery = 32% Analysis Date = 03/28/14 Pct Recovery = 32% Analysis Date = 03/18/14 Pct Recovery = 33% Analysis Date = 03/18/14 Pct Recovery = 33% Analysis Date = 03/08/14 Pct Recovery = 34% Analysis Date = 03/08/14 Pct Recovery = 34% Analysis Date = 02/26/14 Pct Recovery = 35% Analysis Date = 02/26/14 Pct Recovery = 35% Analysis Date = 02/17/14 Pct Recovery = 35% Analysis Date = 02/17/14 Pct Recovery = 35% Analysis Date = 02/07/14 Pct Recovery = 36% Analysis Date = 02/07/14 Pct Recovery = 36% Analysis Date = 01/28/14 Pct Recovery = 37% Analysis Date = 01/28/14 Pct Recovery = 37% Analysis Date = 01/18/14 Pct Recovery = 38% Analysis Date = 01/18/14 Pct Recovery = 38% Analysis Date = 01/08/14 Pct Recovery = 39% Analysis Date = 01/08/14 Pct Recovery = 39% Analysis Date = 12/29/13 Pct Recovery = 39% Analysis Date = 12/29/13 Pct Recovery = 39% Analysis Date = 12/19/13 Pct Recovery = 40% Analysis Date = 12/19/13 Pct Recovery = 40% Analysis Date = 12/09/13 Pct Recovery = 41% Analysis Date = 12/09/13 Pct Recovery = 41% Analysis Date = 11/29/13 Pct Recovery = 42% Analysis Date = 11/29/13 Pct Recovery = 42% Analysis Date = 11/19/13 Pct Recovery = 42% Analysis Date = 11/19/13 Pct Recovery = 42% Analysis Date = 11/10/13 Pct Recovery = 43% Analysis Date = 11/10/13 Pct Recovery = 43% Analysis Date = 10/31/13 Pct Recovery = 44% Analysis Date = 10/31/13 Pct Recovery = 44% Analysis Date = 10/21/13 Pct Recovery = 45% Analysis Date = 10/21/13 Pct Recovery = 45% Analysis Date = 10/11/13 Pct Recovery = 45% Analysis Date = 10/11/13 Pct Recovery = 45% Analysis Date = 10/01/13 Pct Recovery = 46% Analysis Date = 10/01/13 Pct Recovery = 46% Analysis Date = 09/21/13 Pct Recovery = 47% Analysis Date = 09/21/13 Pct Recovery = 47% Analysis Date = 09/11/13 Pct Recovery = 47% Analysis Date = 09/11/13 Pct Recovery = 47% Analysis Date = 09/01/13 Pct Recovery = 48% Analysis Date = 09/01/13 Pct Recovery = 48% Analysis Date = 08/22/13 Pct Recovery = 49% Analysis Date = 08/22/13 Pct Recovery = 49% Analysis Date = 08/12/13 Pct Recovery = 50% Analysis Date = 08/12/13 Pct Recovery = 50% Analysis Date = 08/03/13 Pct Recovery = 50% Analysis Date = 08/03/13 Pct Recovery = 50% Analysis Date = 07/24/13 Pct Recovery = 51% Analysis Date = 07/24/13 Pct Recovery = 51% Analysis Date = 07/14/13 Pct Recovery = 52% Analysis Date = 07/14/13 Pct Recovery = 52% Analysis Date = 07/04/13 Pct Recovery = 53% Analysis Date = 07/04/13 Pct Recovery = 53% Analysis Date = 06/24/13 Pct Recovery = 53% Analysis Date = 06/24/13 Pct Recovery = 53% Analysis Date = 06/14/13 Pct Recovery = 54% Analysis Date = 06/14/13 Pct Recovery = 54% Analysis Date = 06/04/13 Pct Recovery = 55% Analysis Date = 06/04/13 Pct Recovery = 55% Analysis Date = 05/25/13 Pct Recovery = 56% Analysis Date = 05/25/13 Pct Recovery = 56% Analysis Date = 05/15/13 Pct Recovery = 57% Analysis Date = 05/15/13 Pct Recovery = 57% Analysis Date = 05/05/13 Pct Recovery = 57% Analysis Date = 05/05/13 Pct Recovery = 57% Analysis Date = 04/26/13 Pct Recovery = 58% Analysis Date = 04/26/13 Pct Recovery = 58% Analysis Date = 04/16/13 Pct Recovery = 59% Analysis Date = 04/16/13 Pct Recovery = 59% Analysis Date = 04/06/13 Pct Recovery = 60% Analysis Date = 04/06/13 Pct Recovery = 60% Analysis Date = 03/27/13 Pct Recovery = 60% Analysis Date = 03/27/13 Pct Recovery = 60% Analysis Date = 03/17/13 Pct Recovery = 61% Analysis Date = 03/17/13 Pct Recovery = 61% Analysis Date = 03/07/13 Pct Recovery = 62% Analysis Date = 03/07/13 Pct Recovery = 62% Analysis Date = 02/25/13 Pct Recovery = 63% Analysis Date = 02/25/13 Pct Recovery = 63% Analysis Date = 02/15/13 Pct Recovery = 64% Analysis Date = 02/15/13 Pct Recovery = 64% Analysis Date = 02/05/13 Pct Recovery = 64% Analysis Date = 02/05/13 Pct Recovery = 64% Analysis Date = 01/26/13 Pct Recovery = 65% Analysis Date = 01/26/13 Pct Recovery = 65% Analysis Date = 01/17/13 Pct Recovery = 66% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
FENAMIPHOS SULFOXIDE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 72 27% 22% 20% 10%
Total 72 27% 22% 20% 10%

Sample Statistics
FENAMIPHOS SULFOXIDE

Characteristic N % % Basis
Plotted 72 94% Spiked
Estimated Values 72 94% Spiked
Deleted Values 7 6% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 81 .  
False Negatives 5 6% 5 out of 77
Not Spiked 44 .  
False Positives 0 0% 0 out of 41

OBSP Determination:
FIPRONIL
METHOD: 2033 , TESTIDCODE: 62166GCM29

Laboratory ID = 20132490342 Lab Value = 0.220 Expected Conc. = 0.249 Report level label = 0.018 Pct Recovery = 88% Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20132140002 Lab Value = 0.126 Expected Conc. = 0.1249 Report level label = 0.018 Pct Recovery = 101% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl SpecificMix = LB99392 Laboratory ID = 20131370001 Lab Value = 0.142 Expected Conc. = 0.1249 Report level label = 0.018 Pct Recovery = 114% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl SpecificMix = LB99392 Laboratory ID = 20140370077 Lab Value = 0.095 Expected Conc. = 0.1245 Report level label = 0.018 Pct Recovery = 76% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20132560001 Lab Value = 0.117 Expected Conc. = 0.1245 Report level label = 0.018 Pct Recovery = 94% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20172510330 Lab Value = 0.108 Expected Conc. = 0.12 Report level label = 0.018 Pct Recovery = 90% Analysis Date = 12/29/17 SpikeMix = ChemService 6537100: 100 µl & Abs 071817Pest: 100 µl SpecificMix = 071817Pest Laboratory ID = 20162860079 Lab Value = 0.105 Expected Conc. = 0.114 Report level label = 0.018 Pct Recovery = 92% Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl SpecificMix = 060916 Laboratory ID = 20163150006 Lab Value = 0.113 Expected Conc. = 0.114 Report level label = 0.018 Pct Recovery = 99% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl SpecificMix = 060916 Laboratory ID = 20152750006 Lab Value = 0.095 Expected Conc. = 0.108 Report level label = 0.018 Pct Recovery = 88% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl SpecificMix = EN150514012 Laboratory ID = 20152460215 Lab Value = 0.095 Expected Conc. = 0.108 Report level label = 0.018 Pct Recovery = 88% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl SpecificMix = EN150514012 Laboratory ID = 20171660002 Lab Value = 0.088 Expected Conc. = 0.0912 Report level label = 0.018 Pct Recovery = 96% Analysis Date = 08/23/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = 060916 Laboratory ID = 20170190026 Lab Value = 0.086 Expected Conc. = 0.0912 Report level label = 0.018 Pct Recovery = 94% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = 060916 Laboratory ID = 20171380001 Lab Value = 0.077 Expected Conc. = 0.0896 Report level label = 0.018 Pct Recovery = 86% Analysis Date = 06/07/17 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 041816 Laboratory ID = 20170740063 Lab Value = 0.089 Expected Conc. = 0.0896 Report level label = 0.018 Pct Recovery = 100% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl SpecificMix = 041816 Laboratory ID = 20161740258 Lab Value = 0.085 Expected Conc. = 0.0896 Report level label = 0.018 Pct Recovery = 95% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 041816 Laboratory ID = 20130940097 Lab Value = 0.081 Expected Conc. = 0.0755 Report level label = 0.018 Pct Recovery = 107% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = 0507-12-04.2 Laboratory ID = 20123560092 Lab Value = 0.063 Expected Conc. = 0.0755 Report level label = 0.018 Pct Recovery = 83% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = 0507-12-04.2 Laboratory ID = 20130810108 Lab Value = 0.078 Expected Conc. = 0.0751 Report level label = 0.018 Pct Recovery = 104% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl SpecificMix = LB92783 Laboratory ID = 20130100066 Lab Value = 0.078 Expected Conc. = 0.0751 Report level label = 0.018 Pct Recovery = 103% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl SpecificMix = LB92783 Laboratory ID = 20143240095 Lab Value = 0.073 Expected Conc. = 0.0726 Report level label = 0.018 Pct Recovery = 100% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl SpecificMix = 032714 Laboratory ID = 20142270001 Lab Value = 0.064 Expected Conc. = 0.0726 Report level label = 0.018 Pct Recovery = 88% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl SpecificMix = 032714 Laboratory ID = 20141220025 Lab Value = 0.069 Expected Conc. = 0.0726 Report level label = 0.018 Pct Recovery = 94% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl SpecificMix = 032714 Laboratory ID = 20150430092 Lab Value = 0.076 Expected Conc. = 0.072 Report level label = 0.018 Pct Recovery = 106% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl SpecificMix = E1140407002 Laboratory ID = 20143110108 Lab Value = 0.067 Expected Conc. = 0.072 Report level label = 0.018 Pct Recovery = 93% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl SpecificMix = E1140407002 Laboratory ID = 20142720002 Lab Value = 0.073 Expected Conc. = 0.072 Report level label = 0.018 Pct Recovery = 101% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl SpecificMix = E1140407002 Laboratory ID = 20141770149 Lab Value = 0.072 Expected Conc. = 0.072 Report level label = 0.018 Pct Recovery = 100% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl SpecificMix = E1140407002 Laboratory ID = 20181430122 Lab Value = 0.063 Expected Conc. = 0.06 Report level label = 0.018 Pct Recovery = 105% Analysis Date = 06/20/18 SpikeMix = Abs 071817Pest: 50 µl & Spex Organics EN170808006: 50 µl SpecificMix = 071817Pest Laboratory ID = 20173480003 Lab Value = 0.056 Expected Conc. = 0.06 Report level label = 0.018 Pct Recovery = 93% Analysis Date = 04/05/18 SpikeMix = Abs 071717Pest: 50 µl & ChemService 6567600: 50 µl SpecificMix = 6567600 Laboratory ID = 20172560101 Lab Value = 0.056 Expected Conc. = 0.06 Report level label = 0.018 Pct Recovery = 93% Analysis Date = 12/22/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6567600: 50 µl SpecificMix = 6567600 Laboratory ID = 20160630046 Lab Value = 0.060 Expected Conc. = 0.054 Report level label = 0.018 Pct Recovery = 111% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = EN150514012 Laboratory ID = 20153440001 Lab Value = 0.057 Expected Conc. = 0.054 Report level label = 0.018 Pct Recovery = 105% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = EN150514012 Laboratory ID = 20152330039 Lab Value = 0.047 Expected Conc. = 0.054 Report level label = 0.018 Pct Recovery = 86% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl SpecificMix = 041415 Laboratory ID = 20151900132 Lab Value = 0.060 Expected Conc. = 0.054 Report level label = 0.018 Pct Recovery = 111% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl SpecificMix = 041415 Laboratory ID = 20151270112 Lab Value = 0.049 Expected Conc. = 0.054 Report level label = 0.018 Pct Recovery = 91% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl SpecificMix = 041415 Laboratory ID = 20140510043 Lab Value = 0.046 Expected Conc. = 0.05 Report level label = 0.018 Pct Recovery = 91% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl SpecificMix = LB99392 Laboratory ID = 20133470008 Lab Value = 0.048 Expected Conc. = 0.05 Report level label = 0.018 Pct Recovery = 95% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl SpecificMix = LB99392 Laboratory ID = 20133190012 Lab Value = 0.076 Expected Conc. = 0.05 Report level label = 0.018 Pct Recovery = 153% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = LB99392 Laboratory ID = 20133050050 Lab Value = 0.054 Expected Conc. = 0.05 Report level label = 0.018 Pct Recovery = 108% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl SpecificMix = LB99392 Laboratory ID = 20133580036 Lab Value = 0.039 Expected Conc. = 0.0498 Report level label = 0.018 Pct Recovery = 79% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20131790009 Lab Value = 0.024 Expected Conc. = 0.0498 Report level label = 0.018 Pct Recovery = 49% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20131510026 Lab Value = 0.051 Expected Conc. = 0.0498 Report level label = 0.018 Pct Recovery = 101% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20171160110 Lab Value = 0.049 Expected Conc. = 0.0456 Report level label = 0.018 Pct Recovery = 108% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = 060916 Laboratory ID = 20162520001 Lab Value = 0.060 Expected Conc. = 0.0456 Report level label = 0.018 Pct Recovery = 130% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl SpecificMix = 060916 Laboratory ID = 20163560019 Lab Value = 0.048 Expected Conc. = 0.0456 Report level label = 0.018 Pct Recovery = 104% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl SpecificMix = 060916 Laboratory ID = 20162380004 Lab Value = 0.043 Expected Conc. = 0.0456 Report level label = 0.018 Pct Recovery = 95% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = 060916 Laboratory ID = 20171940002 Lab Value = 0.050 Expected Conc. = 0.0448 Report level label = 0.018 Pct Recovery = 111% Analysis Date = 11/10/17 SpikeMix = ChemService 5054800: 40 µl & NSI 041816: 40 µl SpecificMix = 041816 Laboratory ID = 20162020124 Lab Value = 0.045 Expected Conc. = 0.0448 Report level label = 0.018 Pct Recovery = 101% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl SpecificMix = 041816 Laboratory ID = 20161600087 Lab Value = 0.057 Expected Conc. = 0.0448 Report level label = 0.018 Pct Recovery = 126% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 041816 Laboratory ID = 20161340228 Lab Value = 0.061 Expected Conc. = 0.0448 Report level label = 0.018 Pct Recovery = 136% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl SpecificMix = 041816 Laboratory ID = 20161190075 Lab Value = 0.055 Expected Conc. = 0.0448 Report level label = 0.018 Pct Recovery = 123% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 041816 Laboratory ID = 20150150115 Lab Value = 0.050 Expected Conc. = 0.0363 Report level label = 0.018 Pct Recovery = 138% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl SpecificMix = 032714 Laboratory ID = 20142820151 Lab Value = 0.042 Expected Conc. = 0.0363 Report level label = 0.018 Pct Recovery = 115% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl SpecificMix = 032714 Laboratory ID = 20141490205 Lab Value = 0.043 Expected Conc. = 0.0363 Report level label = 0.018 Pct Recovery = 119% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = 032714 Laboratory ID = 20141080004 Lab Value = 0.039 Expected Conc. = 0.0363 Report level label = 0.018 Pct Recovery = 108% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl SpecificMix = 032714 Laboratory ID = 20180730064 Lab Value = 0.050 Expected Conc. = 0.036 Report level label = 0.018 Pct Recovery = 139% Analysis Date = 05/16/18 SpikeMix = Abs 071717Pest: 30 µl & Abs 071817Pest: 30 µl SpecificMix = 071817Pest Laboratory ID = 20180050004 Lab Value = 0.042 Expected Conc. = 0.036 Report level label = 0.018 Pct Recovery = 116% Analysis Date = 04/05/18 SpikeMix = Abs 071817Pest: 30 µl & ChemService 6472100: 30 µl SpecificMix = 071817Pest Laboratory ID = 20172780018 Lab Value = 0.040 Expected Conc. = 0.036 Report level label = 0.018 Pct Recovery = 112% Analysis Date = 02/08/18 SpikeMix = ChemService 6537100: 30 µl & Abs 071817Pest: 30 µl SpecificMix = 071817Pest Laboratory ID = 20142470041 Lab Value = 0.044 Expected Conc. = 0.036 Report level label = 0.018 Pct Recovery = 121% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141910243 Lab Value = 0.034 Expected Conc. = 0.036 Report level label = 0.018 Pct Recovery = 95% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141640076 Lab Value = 0.033 Expected Conc. = 0.036 Report level label = 0.018 Pct Recovery = 91% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141360094 Lab Value = 0.032 Expected Conc. = 0.036 Report level label = 0.018 Pct Recovery = 88% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = E1140407002 Laboratory ID = 20130510051 Lab Value = 0.038 Expected Conc. = 0.0302 Report level label = 0.018 Pct Recovery = 125% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl SpecificMix = 0507-12-04.2 Laboratory ID = 20130390105 Lab Value = 0.033 Expected Conc. = 0.03 Report level label = 0.018 Pct Recovery = 110% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl SpecificMix = LB92783 Laboratory ID = 20161050143 Lab Value = 0.033 Expected Conc. = 0.027 Report level label = 0.018 Pct Recovery = 121% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 041415 Laboratory ID = 20160560044 Lab Value = 0.032 Expected Conc. = 0.027 Report level label = 0.018 Pct Recovery = 118% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl SpecificMix = 041415 Laboratory ID = 20160070059 Lab Value = 0.033 Expected Conc. = 0.027 Report level label = 0.018 Pct Recovery = 122% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = EN150514012 Laboratory ID = 20153160001 Lab Value = 0.029 Expected Conc. = 0.027 Report level label = 0.018 Pct Recovery = 107% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = EN150514012 Laboratory ID = 20152950078 Lab Value = 0.018 Expected Conc. = 0.027 Report level label = 0.018 Pct Recovery = 67% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 041415 Laboratory ID = 20152040177 Lab Value = 0.033 Expected Conc. = 0.027 Report level label = 0.018 Pct Recovery = 123% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl SpecificMix = 041415 Laboratory ID = 20151760208 Lab Value = 0.036 Expected Conc. = 0.027 Report level label = 0.018 Pct Recovery = 133% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl SpecificMix = EN150514012 Laboratory ID = 20151480170 Lab Value = 0.034 Expected Conc. = 0.027 Report level label = 0.018 Pct Recovery = 125% Analysis Date = 06/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150514012 Laboratory ID = 20151210037 Lab Value = 0.030 Expected Conc. = 0.027 Report level label = 0.018 Pct Recovery = 109% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 041415 Analysis Date = 06/19/18 Pct Recovery = 105% Analysis Date = 06/10/18 Pct Recovery = 105% Analysis Date = 06/10/18 Pct Recovery = 105% Analysis Date = 05/31/18 Pct Recovery = 105% Analysis Date = 05/31/18 Pct Recovery = 105% Analysis Date = 05/21/18 Pct Recovery = 105% Analysis Date = 05/21/18 Pct Recovery = 105% Analysis Date = 05/11/18 Pct Recovery = 105% Analysis Date = 05/11/18 Pct Recovery = 105% Analysis Date = 05/01/18 Pct Recovery = 105% Analysis Date = 05/01/18 Pct Recovery = 105% Analysis Date = 04/21/18 Pct Recovery = 105% Analysis Date = 04/21/18 Pct Recovery = 105% Analysis Date = 04/11/18 Pct Recovery = 105% Analysis Date = 04/11/18 Pct Recovery = 105% Analysis Date = 04/01/18 Pct Recovery = 105% Analysis Date = 04/01/18 Pct Recovery = 105% Analysis Date = 03/22/18 Pct Recovery = 105% Analysis Date = 03/22/18 Pct Recovery = 105% Analysis Date = 03/12/18 Pct Recovery = 105% Analysis Date = 03/12/18 Pct Recovery = 105% Analysis Date = 03/02/18 Pct Recovery = 105% Analysis Date = 03/02/18 Pct Recovery = 105% Analysis Date = 02/21/18 Pct Recovery = 105% Analysis Date = 02/21/18 Pct Recovery = 105% Analysis Date = 02/11/18 Pct Recovery = 105% Analysis Date = 02/11/18 Pct Recovery = 105% Analysis Date = 02/01/18 Pct Recovery = 105% Analysis Date = 02/01/18 Pct Recovery = 105% Analysis Date = 01/22/18 Pct Recovery = 105% Analysis Date = 01/22/18 Pct Recovery = 105% Analysis Date = 01/12/18 Pct Recovery = 105% Analysis Date = 01/12/18 Pct Recovery = 105% Analysis Date = 01/02/18 Pct Recovery = 105% Analysis Date = 01/02/18 Pct Recovery = 105% Analysis Date = 12/23/17 Pct Recovery = 105% Analysis Date = 12/23/17 Pct Recovery = 105% Analysis Date = 12/13/17 Pct Recovery = 105% Analysis Date = 12/13/17 Pct Recovery = 105% Analysis Date = 12/03/17 Pct Recovery = 105% Analysis Date = 12/03/17 Pct Recovery = 105% Analysis Date = 11/23/17 Pct Recovery = 105% Analysis Date = 11/23/17 Pct Recovery = 105% Analysis Date = 11/13/17 Pct Recovery = 105% Analysis Date = 11/13/17 Pct Recovery = 105% Analysis Date = 11/04/17 Pct Recovery = 105% Analysis Date = 11/04/17 Pct Recovery = 105% Analysis Date = 10/25/17 Pct Recovery = 105% Analysis Date = 10/25/17 Pct Recovery = 105% Analysis Date = 10/15/17 Pct Recovery = 105% Analysis Date = 10/15/17 Pct Recovery = 105% Analysis Date = 10/05/17 Pct Recovery = 105% Analysis Date = 10/05/17 Pct Recovery = 105% Analysis Date = 09/25/17 Pct Recovery = 105% Analysis Date = 09/25/17 Pct Recovery = 105% Analysis Date = 09/15/17 Pct Recovery = 105% Analysis Date = 09/15/17 Pct Recovery = 105% Analysis Date = 09/05/17 Pct Recovery = 105% Analysis Date = 09/05/17 Pct Recovery = 105% Analysis Date = 08/26/17 Pct Recovery = 105% Analysis Date = 08/26/17 Pct Recovery = 105% Analysis Date = 08/16/17 Pct Recovery = 105% Analysis Date = 08/16/17 Pct Recovery = 105% Analysis Date = 08/06/17 Pct Recovery = 105% Analysis Date = 08/06/17 Pct Recovery = 105% Analysis Date = 07/27/17 Pct Recovery = 105% Analysis Date = 07/27/17 Pct Recovery = 105% Analysis Date = 07/18/17 Pct Recovery = 105% Analysis Date = 07/18/17 Pct Recovery = 105% Analysis Date = 07/08/17 Pct Recovery = 105% Analysis Date = 07/08/17 Pct Recovery = 105% Analysis Date = 06/28/17 Pct Recovery = 105% Analysis Date = 06/28/17 Pct Recovery = 105% Analysis Date = 06/18/17 Pct Recovery = 105% Analysis Date = 06/18/17 Pct Recovery = 105% Analysis Date = 06/08/17 Pct Recovery = 105% Analysis Date = 06/08/17 Pct Recovery = 105% Analysis Date = 05/29/17 Pct Recovery = 105% Analysis Date = 05/29/17 Pct Recovery = 105% Analysis Date = 05/19/17 Pct Recovery = 105% Analysis Date = 05/19/17 Pct Recovery = 105% Analysis Date = 05/09/17 Pct Recovery = 105% Analysis Date = 05/09/17 Pct Recovery = 105% Analysis Date = 04/29/17 Pct Recovery = 105% Analysis Date = 04/29/17 Pct Recovery = 105% Analysis Date = 04/19/17 Pct Recovery = 105% Analysis Date = 04/19/17 Pct Recovery = 105% Analysis Date = 04/09/17 Pct Recovery = 105% Analysis Date = 04/09/17 Pct Recovery = 105% Analysis Date = 03/31/17 Pct Recovery = 105% Analysis Date = 03/31/17 Pct Recovery = 105% Analysis Date = 03/21/17 Pct Recovery = 105% Analysis Date = 03/21/17 Pct Recovery = 105% Analysis Date = 03/11/17 Pct Recovery = 105% Analysis Date = 03/11/17 Pct Recovery = 105% Analysis Date = 03/01/17 Pct Recovery = 105% Analysis Date = 03/01/17 Pct Recovery = 105% Analysis Date = 02/19/17 Pct Recovery = 105% Analysis Date = 02/19/17 Pct Recovery = 105% Analysis Date = 02/09/17 Pct Recovery = 105% Analysis Date = 02/09/17 Pct Recovery = 105% Analysis Date = 01/30/17 Pct Recovery = 105% Analysis Date = 01/30/17 Pct Recovery = 105% Analysis Date = 01/20/17 Pct Recovery = 106% Analysis Date = 01/20/17 Pct Recovery = 106% Analysis Date = 01/10/17 Pct Recovery = 106% Analysis Date = 01/10/17 Pct Recovery = 106% Analysis Date = 12/31/16 Pct Recovery = 106% Analysis Date = 12/31/16 Pct Recovery = 106% Analysis Date = 12/21/16 Pct Recovery = 106% Analysis Date = 12/21/16 Pct Recovery = 106% Analysis Date = 12/12/16 Pct Recovery = 106% Analysis Date = 12/12/16 Pct Recovery = 106% Analysis Date = 12/02/16 Pct Recovery = 106% Analysis Date = 12/02/16 Pct Recovery = 106% Analysis Date = 11/22/16 Pct Recovery = 106% Analysis Date = 11/22/16 Pct Recovery = 106% Analysis Date = 11/12/16 Pct Recovery = 106% Analysis Date = 11/12/16 Pct Recovery = 106% Analysis Date = 11/02/16 Pct Recovery = 106% Analysis Date = 11/02/16 Pct Recovery = 106% Analysis Date = 10/23/16 Pct Recovery = 106% Analysis Date = 10/23/16 Pct Recovery = 106% Analysis Date = 10/13/16 Pct Recovery = 106% Analysis Date = 10/13/16 Pct Recovery = 106% Analysis Date = 10/03/16 Pct Recovery = 106% Analysis Date = 10/03/16 Pct Recovery = 106% Analysis Date = 09/23/16 Pct Recovery = 106% Analysis Date = 09/23/16 Pct Recovery = 106% Analysis Date = 09/13/16 Pct Recovery = 106% Analysis Date = 09/13/16 Pct Recovery = 106% Analysis Date = 09/03/16 Pct Recovery = 106% Analysis Date = 09/03/16 Pct Recovery = 106% Analysis Date = 08/25/16 Pct Recovery = 106% Analysis Date = 08/25/16 Pct Recovery = 106% Analysis Date = 08/15/16 Pct Recovery = 106% Analysis Date = 08/15/16 Pct Recovery = 106% Analysis Date = 08/05/16 Pct Recovery = 106% Analysis Date = 08/05/16 Pct Recovery = 106% Analysis Date = 07/26/16 Pct Recovery = 106% Analysis Date = 07/26/16 Pct Recovery = 106% Analysis Date = 07/16/16 Pct Recovery = 106% Analysis Date = 07/16/16 Pct Recovery = 106% Analysis Date = 07/06/16 Pct Recovery = 106% Analysis Date = 07/06/16 Pct Recovery = 106% Analysis Date = 06/26/16 Pct Recovery = 106% Analysis Date = 06/26/16 Pct Recovery = 106% Analysis Date = 06/16/16 Pct Recovery = 107% Analysis Date = 06/16/16 Pct Recovery = 107% Analysis Date = 06/06/16 Pct Recovery = 107% Analysis Date = 06/06/16 Pct Recovery = 107% Analysis Date = 05/27/16 Pct Recovery = 107% Analysis Date = 05/27/16 Pct Recovery = 107% Analysis Date = 05/17/16 Pct Recovery = 107% Analysis Date = 05/17/16 Pct Recovery = 107% Analysis Date = 05/08/16 Pct Recovery = 107% Analysis Date = 05/08/16 Pct Recovery = 107% Analysis Date = 04/28/16 Pct Recovery = 107% Analysis Date = 04/28/16 Pct Recovery = 107% Analysis Date = 04/18/16 Pct Recovery = 107% Analysis Date = 04/18/16 Pct Recovery = 107% Analysis Date = 04/08/16 Pct Recovery = 107% Analysis Date = 04/08/16 Pct Recovery = 107% Analysis Date = 03/29/16 Pct Recovery = 107% Analysis Date = 03/29/16 Pct Recovery = 107% Analysis Date = 03/19/16 Pct Recovery = 108% Analysis Date = 03/19/16 Pct Recovery = 108% Analysis Date = 03/09/16 Pct Recovery = 108% Analysis Date = 03/09/16 Pct Recovery = 108% Analysis Date = 02/28/16 Pct Recovery = 108% Analysis Date = 02/28/16 Pct Recovery = 108% Analysis Date = 02/18/16 Pct Recovery = 108% Analysis Date = 02/18/16 Pct Recovery = 108% Analysis Date = 02/08/16 Pct Recovery = 108% Analysis Date = 02/08/16 Pct Recovery = 108% Analysis Date = 01/29/16 Pct Recovery = 108% Analysis Date = 01/29/16 Pct Recovery = 108% Analysis Date = 01/20/16 Pct Recovery = 108% Analysis Date = 01/20/16 Pct Recovery = 108% Analysis Date = 01/10/16 Pct Recovery = 108% Analysis Date = 01/10/16 Pct Recovery = 108% Analysis Date = 12/31/15 Pct Recovery = 108% Analysis Date = 12/31/15 Pct Recovery = 108% Analysis Date = 12/21/15 Pct Recovery = 108% Analysis Date = 12/21/15 Pct Recovery = 108% Analysis Date = 12/11/15 Pct Recovery = 108% Analysis Date = 12/11/15 Pct Recovery = 108% Analysis Date = 12/01/15 Pct Recovery = 108% Analysis Date = 12/01/15 Pct Recovery = 108% Analysis Date = 11/21/15 Pct Recovery = 108% Analysis Date = 11/21/15 Pct Recovery = 108% Analysis Date = 11/11/15 Pct Recovery = 108% Analysis Date = 11/11/15 Pct Recovery = 108% Analysis Date = 11/01/15 Pct Recovery = 108% Analysis Date = 11/01/15 Pct Recovery = 108% Analysis Date = 10/22/15 Pct Recovery = 108% Analysis Date = 10/22/15 Pct Recovery = 108% Analysis Date = 10/12/15 Pct Recovery = 108% Analysis Date = 10/12/15 Pct Recovery = 108% Analysis Date = 10/02/15 Pct Recovery = 108% Analysis Date = 10/02/15 Pct Recovery = 108% Analysis Date = 09/23/15 Pct Recovery = 108% Analysis Date = 09/23/15 Pct Recovery = 108% Analysis Date = 09/13/15 Pct Recovery = 108% Analysis Date = 09/13/15 Pct Recovery = 108% Analysis Date = 09/03/15 Pct Recovery = 108% Analysis Date = 09/03/15 Pct Recovery = 108% Analysis Date = 08/24/15 Pct Recovery = 108% Analysis Date = 08/24/15 Pct Recovery = 108% Analysis Date = 08/14/15 Pct Recovery = 108% Analysis Date = 08/14/15 Pct Recovery = 108% Analysis Date = 08/04/15 Pct Recovery = 108% Analysis Date = 08/04/15 Pct Recovery = 108% Analysis Date = 07/25/15 Pct Recovery = 107% Analysis Date = 07/25/15 Pct Recovery = 107% Analysis Date = 07/15/15 Pct Recovery = 107% Analysis Date = 07/15/15 Pct Recovery = 107% Analysis Date = 07/05/15 Pct Recovery = 107% Analysis Date = 07/05/15 Pct Recovery = 107% Analysis Date = 06/25/15 Pct Recovery = 107% Analysis Date = 06/25/15 Pct Recovery = 107% Analysis Date = 06/15/15 Pct Recovery = 107% Analysis Date = 06/15/15 Pct Recovery = 107% Analysis Date = 06/06/15 Pct Recovery = 107% Analysis Date = 06/06/15 Pct Recovery = 107% Analysis Date = 05/27/15 Pct Recovery = 107% Analysis Date = 05/27/15 Pct Recovery = 107% Analysis Date = 05/17/15 Pct Recovery = 106% Analysis Date = 05/17/15 Pct Recovery = 106% Analysis Date = 05/07/15 Pct Recovery = 106% Analysis Date = 05/07/15 Pct Recovery = 106% Analysis Date = 04/27/15 Pct Recovery = 106% Analysis Date = 04/27/15 Pct Recovery = 106% Analysis Date = 04/17/15 Pct Recovery = 106% Analysis Date = 04/17/15 Pct Recovery = 106% Analysis Date = 04/07/15 Pct Recovery = 106% Analysis Date = 04/07/15 Pct Recovery = 106% Analysis Date = 03/28/15 Pct Recovery = 106% Analysis Date = 03/28/15 Pct Recovery = 106% Analysis Date = 03/18/15 Pct Recovery = 105% Analysis Date = 03/18/15 Pct Recovery = 105% Analysis Date = 03/08/15 Pct Recovery = 105% Analysis Date = 03/08/15 Pct Recovery = 105% Analysis Date = 02/26/15 Pct Recovery = 105% Analysis Date = 02/26/15 Pct Recovery = 105% Analysis Date = 02/17/15 Pct Recovery = 105% Analysis Date = 02/17/15 Pct Recovery = 105% Analysis Date = 02/07/15 Pct Recovery = 105% Analysis Date = 02/07/15 Pct Recovery = 105% Analysis Date = 01/28/15 Pct Recovery = 105% Analysis Date = 01/28/15 Pct Recovery = 105% Analysis Date = 01/18/15 Pct Recovery = 105% Analysis Date = 01/18/15 Pct Recovery = 105% Analysis Date = 01/08/15 Pct Recovery = 105% Analysis Date = 01/08/15 Pct Recovery = 105% Analysis Date = 12/29/14 Pct Recovery = 104% Analysis Date = 12/29/14 Pct Recovery = 104% Analysis Date = 12/19/14 Pct Recovery = 104% Analysis Date = 12/19/14 Pct Recovery = 104% Analysis Date = 12/09/14 Pct Recovery = 104% Analysis Date = 12/09/14 Pct Recovery = 104% Analysis Date = 11/29/14 Pct Recovery = 104% Analysis Date = 11/29/14 Pct Recovery = 104% Analysis Date = 11/19/14 Pct Recovery = 104% Analysis Date = 11/19/14 Pct Recovery = 104% Analysis Date = 11/09/14 Pct Recovery = 104% Analysis Date = 11/09/14 Pct Recovery = 104% Analysis Date = 10/31/14 Pct Recovery = 104% Analysis Date = 10/31/14 Pct Recovery = 104% Analysis Date = 10/21/14 Pct Recovery = 104% Analysis Date = 10/21/14 Pct Recovery = 104% Analysis Date = 10/11/14 Pct Recovery = 104% Analysis Date = 10/11/14 Pct Recovery = 104% Analysis Date = 10/01/14 Pct Recovery = 104% Analysis Date = 10/01/14 Pct Recovery = 104% Analysis Date = 09/21/14 Pct Recovery = 103% Analysis Date = 09/21/14 Pct Recovery = 103% Analysis Date = 09/11/14 Pct Recovery = 103% Analysis Date = 09/11/14 Pct Recovery = 103% Analysis Date = 09/01/14 Pct Recovery = 103% Analysis Date = 09/01/14 Pct Recovery = 103% Analysis Date = 08/22/14 Pct Recovery = 103% Analysis Date = 08/22/14 Pct Recovery = 103% Analysis Date = 08/12/14 Pct Recovery = 103% Analysis Date = 08/12/14 Pct Recovery = 103% Analysis Date = 08/02/14 Pct Recovery = 103% Analysis Date = 08/02/14 Pct Recovery = 103% Analysis Date = 07/23/14 Pct Recovery = 102% Analysis Date = 07/23/14 Pct Recovery = 102% Analysis Date = 07/14/14 Pct Recovery = 102% Analysis Date = 07/14/14 Pct Recovery = 102% Analysis Date = 07/04/14 Pct Recovery = 102% Analysis Date = 07/04/14 Pct Recovery = 102% Analysis Date = 06/24/14 Pct Recovery = 102% Analysis Date = 06/24/14 Pct Recovery = 102% Analysis Date = 06/14/14 Pct Recovery = 102% Analysis Date = 06/14/14 Pct Recovery = 102% Analysis Date = 06/04/14 Pct Recovery = 102% Analysis Date = 06/04/14 Pct Recovery = 102% Analysis Date = 05/25/14 Pct Recovery = 102% Analysis Date = 05/25/14 Pct Recovery = 102% Analysis Date = 05/15/14 Pct Recovery = 102% Analysis Date = 05/15/14 Pct Recovery = 102% Analysis Date = 05/05/14 Pct Recovery = 102% Analysis Date = 05/05/14 Pct Recovery = 102% Analysis Date = 04/25/14 Pct Recovery = 102% Analysis Date = 04/25/14 Pct Recovery = 102% Analysis Date = 04/15/14 Pct Recovery = 101% Analysis Date = 04/15/14 Pct Recovery = 101% Analysis Date = 04/05/14 Pct Recovery = 101% Analysis Date = 04/05/14 Pct Recovery = 101% Analysis Date = 03/27/14 Pct Recovery = 101% Analysis Date = 03/27/14 Pct Recovery = 101% Analysis Date = 03/17/14 Pct Recovery = 101% Analysis Date = 03/17/14 Pct Recovery = 101% Analysis Date = 03/07/14 Pct Recovery = 101% Analysis Date = 03/07/14 Pct Recovery = 101% Analysis Date = 02/25/14 Pct Recovery = 101% Analysis Date = 02/25/14 Pct Recovery = 101% Analysis Date = 02/15/14 Pct Recovery = 101% Analysis Date = 02/15/14 Pct Recovery = 101% Analysis Date = 02/05/14 Pct Recovery = 101% Analysis Date = 02/05/14 Pct Recovery = 101% Analysis Date = 01/26/14 Pct Recovery = 101% Analysis Date = 01/26/14 Pct Recovery = 101% Analysis Date = 01/16/14 Pct Recovery = 101% Analysis Date = 01/16/14 Pct Recovery = 101% Analysis Date = 01/06/14 Pct Recovery = 101% Analysis Date = 01/06/14 Pct Recovery = 101% Analysis Date = 12/27/13 Pct Recovery = 101% Analysis Date = 12/27/13 Pct Recovery = 101% Analysis Date = 12/17/13 Pct Recovery = 101% Analysis Date = 12/17/13 Pct Recovery = 101% Analysis Date = 12/08/13 Pct Recovery = 100% Analysis Date = 12/08/13 Pct Recovery = 100% Analysis Date = 11/28/13 Pct Recovery = 100% Analysis Date = 11/28/13 Pct Recovery = 100% Analysis Date = 11/18/13 Pct Recovery = 100% Analysis Date = 11/18/13 Pct Recovery = 100% Analysis Date = 11/08/13 Pct Recovery = 100% Analysis Date = 11/08/13 Pct Recovery = 100% Analysis Date = 10/29/13 Pct Recovery = 100% Analysis Date = 10/29/13 Pct Recovery = 100% Analysis Date = 10/19/13 Pct Recovery = 100% Analysis Date = 10/19/13 Pct Recovery = 100% Analysis Date = 10/09/13 Pct Recovery = 100% Analysis Date = 10/09/13 Pct Recovery = 100% Analysis Date = 09/29/13 Pct Recovery = 100% Analysis Date = 09/29/13 Pct Recovery = 100% Analysis Date = 09/19/13 Pct Recovery = 100% Analysis Date = 09/19/13 Pct Recovery = 100% Analysis Date = 09/09/13 Pct Recovery = 100% Analysis Date = 09/09/13 Pct Recovery = 100% Analysis Date = 08/30/13 Pct Recovery = 100% Analysis Date = 08/30/13 Pct Recovery = 100% Analysis Date = 08/21/13 Pct Recovery = 100% Analysis Date = 08/21/13 Pct Recovery = 100% Analysis Date = 08/11/13 Pct Recovery = 100% Analysis Date = 08/11/13 Pct Recovery = 100% Analysis Date = 08/01/13 Pct Recovery = 100% Analysis Date = 08/01/13 Pct Recovery = 100% Analysis Date = 07/22/13 Pct Recovery = 100% Analysis Date = 07/22/13 Pct Recovery = 100% Analysis Date = 07/12/13 Pct Recovery = 100% Analysis Date = 07/12/13 Pct Recovery = 100% Analysis Date = 07/02/13 Pct Recovery = 100% Analysis Date = 07/02/13 Pct Recovery = 100% Analysis Date = 06/22/13 Pct Recovery = 100% Analysis Date = 06/22/13 Pct Recovery = 100% Analysis Date = 06/12/13 Pct Recovery = 99% Analysis Date = 06/12/13 Pct Recovery = 99% Analysis Date = 06/02/13 Pct Recovery = 99% Analysis Date = 06/02/13 Pct Recovery = 99% Analysis Date = 05/23/13 Pct Recovery = 99% Analysis Date = 05/23/13 Pct Recovery = 99% Analysis Date = 05/13/13 Pct Recovery = 99% Analysis Date = 05/13/13 Pct Recovery = 99% Analysis Date = 05/04/13 Pct Recovery = 99% Analysis Date = 05/04/13 Pct Recovery = 99% Analysis Date = 04/24/13 Pct Recovery = 99% Analysis Date = 04/24/13 Pct Recovery = 99% Analysis Date = 04/14/13 Pct Recovery = 99% Analysis Date = 04/14/13 Pct Recovery = 99% Analysis Date = 04/04/13 Pct Recovery = 99% Analysis Date = 04/04/13 Pct Recovery = 99% Analysis Date = 03/25/13 Pct Recovery = 99% Analysis Date = 03/25/13 Pct Recovery = 99% Analysis Date = 03/15/13 Pct Recovery = 99% Analysis Date = 03/15/13 Pct Recovery = 99% Analysis Date = 03/05/13 Pct Recovery = 99% Analysis Date = 03/05/13 Pct Recovery = 99% Analysis Date = 02/23/13 Pct Recovery = 99% Analysis Date = 02/23/13 Pct Recovery = 99% Analysis Date = 02/13/13 Pct Recovery = 99% Analysis Date = 02/13/13 Pct Recovery = 99% Analysis Date = 02/03/13 Pct Recovery = 99% Analysis Date = 02/03/13 Pct Recovery = 99% Analysis Date = 01/24/13 Pct Recovery = 99% Analysis Date = 01/24/13 Pct Recovery = 99% Analysis Date = 01/15/13 Pct Recovery = 99% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
FIPRONIL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 72 104% 17% 102% 16%
Total 72 104% 17% 102% 16%

Sample Statistics
FIPRONIL

Characteristic N % % Basis
Plotted 72 99% Spiked
Estimated Values 72 99% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 73 .  
False Negatives 1 1% 1 out of 73
Not Spiked 61 .  
False Positives 0 0% 0 out of 61

OBSP Determination:
FIPRONIL SULFIDE
METHOD: 2033 , TESTIDCODE: 62167GCM29

Laboratory ID = 20132490342 Lab Value = 0.234 Expected Conc. = 0.246 Report level label = 0.016 Pct Recovery = 95% Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20132140002 Lab Value = 0.119 Expected Conc. = 0.125 Report level label = 0.016 Pct Recovery = 95% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl SpecificMix = LB99392 Laboratory ID = 20131370001 Lab Value = 0.142 Expected Conc. = 0.125 Report level label = 0.016 Pct Recovery = 114% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl SpecificMix = LB99392 Laboratory ID = 20140370077 Lab Value = 0.097 Expected Conc. = 0.123 Report level label = 0.016 Pct Recovery = 79% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20132560001 Lab Value = 0.111 Expected Conc. = 0.123 Report level label = 0.016 Pct Recovery = 90% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20172510330 Lab Value = 0.097 Expected Conc. = 0.107 Report level label = 0.016 Pct Recovery = 91% Analysis Date = 12/29/17 SpikeMix = ChemService 6537100: 100 µl & Abs 071817Pest: 100 µl SpecificMix = 071817Pest Laboratory ID = 20163370001 Lab Value = 0.076 Expected Conc. = 0.1005 Report level label = 0.016 Pct Recovery = 75% Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl SpecificMix = LC20138V Laboratory ID = 20162860079 Lab Value = 0.094 Expected Conc. = 0.1 Report level label = 0.016 Pct Recovery = 94% Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl SpecificMix = 5054800 Laboratory ID = 20161880109 Lab Value = 0.109 Expected Conc. = 0.1 Report level label = 0.016 Pct Recovery = 109% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl SpecificMix = 5054800 Laboratory ID = 20152750006 Lab Value = 0.085 Expected Conc. = 0.096 Report level label = 0.016 Pct Recovery = 88% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl SpecificMix = 040615 Laboratory ID = 20152610011 Lab Value = 0.087 Expected Conc. = 0.096 Report level label = 0.016 Pct Recovery = 91% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl SpecificMix = 040615 Laboratory ID = 20171720140 Lab Value = 0.068 Expected Conc. = 0.0804 Report level label = 0.016 Pct Recovery = 85% Analysis Date = 08/31/17 SpikeMix = Supelco LC20138V: 80 µl & Phenova B20160331: 80 µl SpecificMix = LC20138V Laboratory ID = 20170740063 Lab Value = 0.069 Expected Conc. = 0.0804 Report level label = 0.016 Pct Recovery = 86% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl SpecificMix = LC20138V Laboratory ID = 20161470001 Lab Value = 0.083 Expected Conc. = 0.0804 Report level label = 0.016 Pct Recovery = 103% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl SpecificMix = LC20138V Laboratory ID = 20171380001 Lab Value = 0.059 Expected Conc. = 0.08 Report level label = 0.016 Pct Recovery = 73% Analysis Date = 06/07/17 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 5054800 Laboratory ID = 20170960001 Lab Value = 0.064 Expected Conc. = 0.08 Report level label = 0.016 Pct Recovery = 80% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl SpecificMix = 5054800 Laboratory ID = 20161740258 Lab Value = 0.059 Expected Conc. = 0.08 Report level label = 0.016 Pct Recovery = 73% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 5054800 Laboratory ID = 20130940097 Lab Value = 0.073 Expected Conc. = 0.0765 Report level label = 0.016 Pct Recovery = 96% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = 0507-12-04.2 Laboratory ID = 20123560092 Lab Value = 0.061 Expected Conc. = 0.0765 Report level label = 0.016 Pct Recovery = 80% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = 0507-12-04.2 Laboratory ID = 20130810108 Lab Value = 0.068 Expected Conc. = 0.075 Report level label = 0.016 Pct Recovery = 91% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl SpecificMix = LB92783 Laboratory ID = 20130100066 Lab Value = 0.076 Expected Conc. = 0.075 Report level label = 0.016 Pct Recovery = 101% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl SpecificMix = LB92783 Laboratory ID = 20150430092 Lab Value = 0.060 Expected Conc. = 0.066 Report level label = 0.016 Pct Recovery = 90% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl SpecificMix = E1140407002 Laboratory ID = 20143110108 Lab Value = 0.052 Expected Conc. = 0.066 Report level label = 0.016 Pct Recovery = 79% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl SpecificMix = E1140407002 Laboratory ID = 20142720002 Lab Value = 0.057 Expected Conc. = 0.066 Report level label = 0.016 Pct Recovery = 87% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl SpecificMix = E1140407002 Laboratory ID = 20141770149 Lab Value = 0.057 Expected Conc. = 0.066 Report level label = 0.016 Pct Recovery = 86% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl SpecificMix = E1140407002 Laboratory ID = 20143240095 Lab Value = 0.064 Expected Conc. = 0.0642 Report level label = 0.016 Pct Recovery = 99% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl SpecificMix = 032714 Laboratory ID = 20142270001 Lab Value = 0.051 Expected Conc. = 0.0642 Report level label = 0.016 Pct Recovery = 79% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl SpecificMix = 032714 Laboratory ID = 20141220025 Lab Value = 0.067 Expected Conc. = 0.0642 Report level label = 0.016 Pct Recovery = 105% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl SpecificMix = 032714 Laboratory ID = 20172560101 Lab Value = 0.047 Expected Conc. = 0.055 Report level label = 0.016 Pct Recovery = 85% Analysis Date = 12/22/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6567600: 50 µl SpecificMix = 6567600 Laboratory ID = 20140510043 Lab Value = 0.037 Expected Conc. = 0.05 Report level label = 0.016 Pct Recovery = 73% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl SpecificMix = LB99392 Laboratory ID = 20133470008 Lab Value = 0.046 Expected Conc. = 0.05 Report level label = 0.016 Pct Recovery = 92% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl SpecificMix = LB99392 Laboratory ID = 20133190012 Lab Value = 0.056 Expected Conc. = 0.05 Report level label = 0.016 Pct Recovery = 112% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = LB99392 Laboratory ID = 20133050050 Lab Value = 0.042 Expected Conc. = 0.05 Report level label = 0.016 Pct Recovery = 85% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl SpecificMix = LB99392 Laboratory ID = 20133580036 Lab Value = 0.036 Expected Conc. = 0.0492 Report level label = 0.016 Pct Recovery = 73% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20131790009 Lab Value = 0.033 Expected Conc. = 0.0492 Report level label = 0.016 Pct Recovery = 67% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20131510026 Lab Value = 0.052 Expected Conc. = 0.0492 Report level label = 0.016 Pct Recovery = 106% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20161260151 Lab Value = 0.042 Expected Conc. = 0.048 Report level label = 0.016 Pct Recovery = 87% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = EN150513008 Laboratory ID = 20160770090 Lab Value = 0.043 Expected Conc. = 0.048 Report level label = 0.016 Pct Recovery = 89% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = EN150513008 Laboratory ID = 20153510109 Lab Value = 0.039 Expected Conc. = 0.048 Report level label = 0.016 Pct Recovery = 81% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = EN150513008 Laboratory ID = 20152330039 Lab Value = 0.033 Expected Conc. = 0.048 Report level label = 0.016 Pct Recovery = 68% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl SpecificMix = EN150513008 Laboratory ID = 20151900132 Lab Value = 0.049 Expected Conc. = 0.048 Report level label = 0.016 Pct Recovery = 101% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl SpecificMix = 040615 Laboratory ID = 20151550293 Lab Value = 0.044 Expected Conc. = 0.048 Report level label = 0.016 Pct Recovery = 92% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl SpecificMix = 040615 Laboratory ID = 20171510080 Lab Value = 0.039 Expected Conc. = 0.0402 Report level label = 0.016 Pct Recovery = 98% Analysis Date = 06/09/17 SpikeMix = Supelco LC20138V: 40 µl & Crescent 03FF076: 40 µl SpecificMix = LC20138V Laboratory ID = 20162520001 Lab Value = 0.046 Expected Conc. = 0.0402 Report level label = 0.016 Pct Recovery = 113% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl SpecificMix = LC20138V Laboratory ID = 20162660005 Lab Value = 0.037 Expected Conc. = 0.0402 Report level label = 0.016 Pct Recovery = 92% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl SpecificMix = LC20138V Laboratory ID = 20162020124 Lab Value = 0.036 Expected Conc. = 0.0402 Report level label = 0.016 Pct Recovery = 89% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl SpecificMix = LC20138V Laboratory ID = 20171940002 Lab Value = 0.040 Expected Conc. = 0.04 Report level label = 0.016 Pct Recovery = 99% Analysis Date = 11/10/17 SpikeMix = ChemService 5054800: 40 µl & NSI 041816: 40 µl SpecificMix = 5054800 Laboratory ID = 20170460061 Lab Value = 0.034 Expected Conc. = 0.04 Report level label = 0.016 Pct Recovery = 85% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl SpecificMix = 5054800 Laboratory ID = 20163560019 Lab Value = 0.034 Expected Conc. = 0.04 Report level label = 0.016 Pct Recovery = 84% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl SpecificMix = 5054800 Laboratory ID = 20162150213 Lab Value = 0.038 Expected Conc. = 0.04 Report level label = 0.016 Pct Recovery = 94% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl SpecificMix = 5054800 Laboratory ID = 20142470041 Lab Value = 0.035 Expected Conc. = 0.033 Report level label = 0.016 Pct Recovery = 107% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141910243 Lab Value = 0.027 Expected Conc. = 0.033 Report level label = 0.016 Pct Recovery = 82% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141640076 Lab Value = 0.026 Expected Conc. = 0.033 Report level label = 0.016 Pct Recovery = 78% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141360094 Lab Value = 0.023 Expected Conc. = 0.033 Report level label = 0.016 Pct Recovery = 69% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = E1140407002 Laboratory ID = 20172780018 Lab Value = 0.033 Expected Conc. = 0.0321 Report level label = 0.016 Pct Recovery = 101% Analysis Date = 02/08/18 SpikeMix = ChemService 6537100: 30 µl & Abs 071817Pest: 30 µl SpecificMix = 071817Pest Laboratory ID = 20150150115 Lab Value = 0.032 Expected Conc. = 0.0321 Report level label = 0.016 Pct Recovery = 98% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl SpecificMix = 032714 Laboratory ID = 20142820151 Lab Value = 0.034 Expected Conc. = 0.0321 Report level label = 0.016 Pct Recovery = 104% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl SpecificMix = 032714 Laboratory ID = 20141490205 Lab Value = 0.037 Expected Conc. = 0.0321 Report level label = 0.016 Pct Recovery = 114% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = 032714 Laboratory ID = 20141080004 Lab Value = 0.032 Expected Conc. = 0.0321 Report level label = 0.016 Pct Recovery = 98% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl SpecificMix = 032714 Laboratory ID = 20130510051 Lab Value = 0.030 Expected Conc. = 0.0306 Report level label = 0.016 Pct Recovery = 97% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl SpecificMix = 0507-12-04.2 Laboratory ID = 20130390105 Lab Value = 0.027 Expected Conc. = 0.03 Report level label = 0.016 Pct Recovery = 90% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl SpecificMix = LB92783 Laboratory ID = 20161050143 Lab Value = 0.024 Expected Conc. = 0.024 Report level label = 0.016 Pct Recovery = 102% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Laboratory ID = 20160430111 Lab Value = 0.027 Expected Conc. = 0.024 Report level label = 0.016 Pct Recovery = 110% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Laboratory ID = 20160560044 Lab Value = 0.023 Expected Conc. = 0.024 Report level label = 0.016 Pct Recovery = 97% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl SpecificMix = EN150513008 Laboratory ID = 20160070059 Lab Value = 0.025 Expected Conc. = 0.024 Report level label = 0.016 Pct Recovery = 104% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = 040615 Laboratory ID = 20153160001 Lab Value = 0.021 Expected Conc. = 0.024 Report level label = 0.016 Pct Recovery = 85% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = EN150513008 Laboratory ID = 20153030068 Lab Value = 0.021 Expected Conc. = 0.024 Report level label = 0.016 Pct Recovery = 88% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150513008 Laboratory ID = 20152190003 Lab Value = 0.018 Expected Conc. = 0.024 Report level label = 0.016 Pct Recovery = 75% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150513008 Laboratory ID = 20151480170 Lab Value = 0.024 Expected Conc. = 0.024 Report level label = 0.016 Pct Recovery = 101% Analysis Date = 06/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150513008 Laboratory ID = 20151380009 Lab Value = 0.024 Expected Conc. = 0.024 Report level label = 0.016 Pct Recovery = 98% Analysis Date = 05/30/15 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Laboratory ID = 20151210037 Lab Value = 0.023 Expected Conc. = 0.024 Report level label = 0.016 Pct Recovery = 97% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Analysis Date = 02/08/18 Pct Recovery = 90% Analysis Date = 01/29/18 Pct Recovery = 90% Analysis Date = 01/29/18 Pct Recovery = 90% Analysis Date = 01/20/18 Pct Recovery = 90% Analysis Date = 01/20/18 Pct Recovery = 90% Analysis Date = 01/11/18 Pct Recovery = 90% Analysis Date = 01/11/18 Pct Recovery = 90% Analysis Date = 01/02/18 Pct Recovery = 90% Analysis Date = 01/02/18 Pct Recovery = 90% Analysis Date = 12/23/17 Pct Recovery = 90% Analysis Date = 12/23/17 Pct Recovery = 90% Analysis Date = 12/14/17 Pct Recovery = 90% Analysis Date = 12/14/17 Pct Recovery = 90% Analysis Date = 12/05/17 Pct Recovery = 90% Analysis Date = 12/05/17 Pct Recovery = 90% Analysis Date = 11/26/17 Pct Recovery = 90% Analysis Date = 11/26/17 Pct Recovery = 90% Analysis Date = 11/16/17 Pct Recovery = 90% Analysis Date = 11/16/17 Pct Recovery = 90% Analysis Date = 11/07/17 Pct Recovery = 90% Analysis Date = 11/07/17 Pct Recovery = 90% Analysis Date = 10/29/17 Pct Recovery = 90% Analysis Date = 10/29/17 Pct Recovery = 90% Analysis Date = 10/20/17 Pct Recovery = 90% Analysis Date = 10/20/17 Pct Recovery = 90% Analysis Date = 10/10/17 Pct Recovery = 90% Analysis Date = 10/10/17 Pct Recovery = 90% Analysis Date = 10/01/17 Pct Recovery = 90% Analysis Date = 10/01/17 Pct Recovery = 90% Analysis Date = 09/22/17 Pct Recovery = 90% Analysis Date = 09/22/17 Pct Recovery = 90% Analysis Date = 09/13/17 Pct Recovery = 90% Analysis Date = 09/13/17 Pct Recovery = 90% Analysis Date = 09/03/17 Pct Recovery = 91% Analysis Date = 09/03/17 Pct Recovery = 91% Analysis Date = 08/25/17 Pct Recovery = 91% Analysis Date = 08/25/17 Pct Recovery = 91% Analysis Date = 08/16/17 Pct Recovery = 91% Analysis Date = 08/16/17 Pct Recovery = 91% Analysis Date = 08/07/17 Pct Recovery = 91% Analysis Date = 08/07/17 Pct Recovery = 91% Analysis Date = 07/28/17 Pct Recovery = 91% Analysis Date = 07/28/17 Pct Recovery = 91% Analysis Date = 07/19/17 Pct Recovery = 91% Analysis Date = 07/19/17 Pct Recovery = 91% Analysis Date = 07/10/17 Pct Recovery = 91% Analysis Date = 07/10/17 Pct Recovery = 91% Analysis Date = 07/01/17 Pct Recovery = 91% Analysis Date = 07/01/17 Pct Recovery = 91% Analysis Date = 06/21/17 Pct Recovery = 91% Analysis Date = 06/21/17 Pct Recovery = 91% Analysis Date = 06/12/17 Pct Recovery = 91% Analysis Date = 06/12/17 Pct Recovery = 91% Analysis Date = 06/03/17 Pct Recovery = 91% Analysis Date = 06/03/17 Pct Recovery = 91% Analysis Date = 05/25/17 Pct Recovery = 91% Analysis Date = 05/25/17 Pct Recovery = 91% Analysis Date = 05/15/17 Pct Recovery = 91% Analysis Date = 05/15/17 Pct Recovery = 91% Analysis Date = 05/06/17 Pct Recovery = 91% Analysis Date = 05/06/17 Pct Recovery = 91% Analysis Date = 04/27/17 Pct Recovery = 91% Analysis Date = 04/27/17 Pct Recovery = 91% Analysis Date = 04/18/17 Pct Recovery = 91% Analysis Date = 04/18/17 Pct Recovery = 91% Analysis Date = 04/08/17 Pct Recovery = 91% Analysis Date = 04/08/17 Pct Recovery = 91% Analysis Date = 03/30/17 Pct Recovery = 91% Analysis Date = 03/30/17 Pct Recovery = 91% Analysis Date = 03/21/17 Pct Recovery = 91% Analysis Date = 03/21/17 Pct Recovery = 91% Analysis Date = 03/12/17 Pct Recovery = 91% Analysis Date = 03/12/17 Pct Recovery = 91% Analysis Date = 03/02/17 Pct Recovery = 91% Analysis Date = 03/02/17 Pct Recovery = 91% Analysis Date = 02/21/17 Pct Recovery = 91% Analysis Date = 02/21/17 Pct Recovery = 91% Analysis Date = 02/12/17 Pct Recovery = 91% Analysis Date = 02/12/17 Pct Recovery = 91% Analysis Date = 02/03/17 Pct Recovery = 91% Analysis Date = 02/03/17 Pct Recovery = 91% Analysis Date = 01/24/17 Pct Recovery = 91% Analysis Date = 01/24/17 Pct Recovery = 91% Analysis Date = 01/15/17 Pct Recovery = 91% Analysis Date = 01/15/17 Pct Recovery = 91% Analysis Date = 01/06/17 Pct Recovery = 91% Analysis Date = 01/06/17 Pct Recovery = 91% Analysis Date = 12/28/16 Pct Recovery = 91% Analysis Date = 12/28/16 Pct Recovery = 91% Analysis Date = 12/18/16 Pct Recovery = 91% Analysis Date = 12/18/16 Pct Recovery = 91% Analysis Date = 12/09/16 Pct Recovery = 91% Analysis Date = 12/09/16 Pct Recovery = 91% Analysis Date = 11/30/16 Pct Recovery = 91% Analysis Date = 11/30/16 Pct Recovery = 91% Analysis Date = 11/21/16 Pct Recovery = 91% Analysis Date = 11/21/16 Pct Recovery = 91% Analysis Date = 11/11/16 Pct Recovery = 91% Analysis Date = 11/11/16 Pct Recovery = 91% Analysis Date = 11/02/16 Pct Recovery = 91% Analysis Date = 11/02/16 Pct Recovery = 91% Analysis Date = 10/24/16 Pct Recovery = 91% Analysis Date = 10/24/16 Pct Recovery = 91% Analysis Date = 10/15/16 Pct Recovery = 91% Analysis Date = 10/15/16 Pct Recovery = 91% Analysis Date = 10/05/16 Pct Recovery = 91% Analysis Date = 10/05/16 Pct Recovery = 91% Analysis Date = 09/26/16 Pct Recovery = 91% Analysis Date = 09/26/16 Pct Recovery = 91% Analysis Date = 09/17/16 Pct Recovery = 91% Analysis Date = 09/17/16 Pct Recovery = 91% Analysis Date = 09/08/16 Pct Recovery = 91% Analysis Date = 09/08/16 Pct Recovery = 91% Analysis Date = 08/29/16 Pct Recovery = 91% Analysis Date = 08/29/16 Pct Recovery = 91% Analysis Date = 08/20/16 Pct Recovery = 91% Analysis Date = 08/20/16 Pct Recovery = 91% Analysis Date = 08/11/16 Pct Recovery = 91% Analysis Date = 08/11/16 Pct Recovery = 91% Analysis Date = 08/02/16 Pct Recovery = 91% Analysis Date = 08/02/16 Pct Recovery = 91% Analysis Date = 07/23/16 Pct Recovery = 91% Analysis Date = 07/23/16 Pct Recovery = 91% Analysis Date = 07/14/16 Pct Recovery = 91% Analysis Date = 07/14/16 Pct Recovery = 91% Analysis Date = 07/05/16 Pct Recovery = 91% Analysis Date = 07/05/16 Pct Recovery = 91% Analysis Date = 06/26/16 Pct Recovery = 91% Analysis Date = 06/26/16 Pct Recovery = 91% Analysis Date = 06/16/16 Pct Recovery = 91% Analysis Date = 06/16/16 Pct Recovery = 91% Analysis Date = 06/07/16 Pct Recovery = 91% Analysis Date = 06/07/16 Pct Recovery = 91% Analysis Date = 05/29/16 Pct Recovery = 91% Analysis Date = 05/29/16 Pct Recovery = 91% Analysis Date = 05/20/16 Pct Recovery = 91% Analysis Date = 05/20/16 Pct Recovery = 91% Analysis Date = 05/10/16 Pct Recovery = 91% Analysis Date = 05/10/16 Pct Recovery = 91% Analysis Date = 05/01/16 Pct Recovery = 92% Analysis Date = 05/01/16 Pct Recovery = 92% Analysis Date = 04/22/16 Pct Recovery = 92% Analysis Date = 04/22/16 Pct Recovery = 92% Analysis Date = 04/13/16 Pct Recovery = 92% Analysis Date = 04/13/16 Pct Recovery = 92% Analysis Date = 04/03/16 Pct Recovery = 92% Analysis Date = 04/03/16 Pct Recovery = 92% Analysis Date = 03/25/16 Pct Recovery = 92% Analysis Date = 03/25/16 Pct Recovery = 92% Analysis Date = 03/16/16 Pct Recovery = 92% Analysis Date = 03/16/16 Pct Recovery = 92% Analysis Date = 03/07/16 Pct Recovery = 92% Analysis Date = 03/07/16 Pct Recovery = 92% Analysis Date = 02/26/16 Pct Recovery = 92% Analysis Date = 02/26/16 Pct Recovery = 92% Analysis Date = 02/17/16 Pct Recovery = 92% Analysis Date = 02/17/16 Pct Recovery = 92% Analysis Date = 02/08/16 Pct Recovery = 92% Analysis Date = 02/08/16 Pct Recovery = 92% Analysis Date = 01/30/16 Pct Recovery = 92% Analysis Date = 01/30/16 Pct Recovery = 92% Analysis Date = 01/20/16 Pct Recovery = 92% Analysis Date = 01/20/16 Pct Recovery = 92% Analysis Date = 01/11/16 Pct Recovery = 92% Analysis Date = 01/11/16 Pct Recovery = 92% Analysis Date = 01/02/16 Pct Recovery = 92% Analysis Date = 01/02/16 Pct Recovery = 92% Analysis Date = 12/24/15 Pct Recovery = 92% Analysis Date = 12/24/15 Pct Recovery = 92% Analysis Date = 12/14/15 Pct Recovery = 92% Analysis Date = 12/14/15 Pct Recovery = 92% Analysis Date = 12/05/15 Pct Recovery = 92% Analysis Date = 12/05/15 Pct Recovery = 92% Analysis Date = 11/26/15 Pct Recovery = 92% Analysis Date = 11/26/15 Pct Recovery = 92% Analysis Date = 11/17/15 Pct Recovery = 92% Analysis Date = 11/17/15 Pct Recovery = 92% Analysis Date = 11/07/15 Pct Recovery = 92% Analysis Date = 11/07/15 Pct Recovery = 92% Analysis Date = 10/29/15 Pct Recovery = 92% Analysis Date = 10/29/15 Pct Recovery = 92% Analysis Date = 10/20/15 Pct Recovery = 92% Analysis Date = 10/20/15 Pct Recovery = 92% Analysis Date = 10/11/15 Pct Recovery = 92% Analysis Date = 10/11/15 Pct Recovery = 92% Analysis Date = 10/01/15 Pct Recovery = 92% Analysis Date = 10/01/15 Pct Recovery = 92% Analysis Date = 09/22/15 Pct Recovery = 92% Analysis Date = 09/22/15 Pct Recovery = 92% Analysis Date = 09/13/15 Pct Recovery = 92% Analysis Date = 09/13/15 Pct Recovery = 92% Analysis Date = 09/04/15 Pct Recovery = 92% Analysis Date = 09/04/15 Pct Recovery = 92% Analysis Date = 08/25/15 Pct Recovery = 92% Analysis Date = 08/25/15 Pct Recovery = 92% Analysis Date = 08/16/15 Pct Recovery = 92% Analysis Date = 08/16/15 Pct Recovery = 92% Analysis Date = 08/07/15 Pct Recovery = 92% Analysis Date = 08/07/15 Pct Recovery = 92% Analysis Date = 07/29/15 Pct Recovery = 92% Analysis Date = 07/29/15 Pct Recovery = 92% Analysis Date = 07/19/15 Pct Recovery = 92% Analysis Date = 07/19/15 Pct Recovery = 92% Analysis Date = 07/10/15 Pct Recovery = 92% Analysis Date = 07/10/15 Pct Recovery = 92% Analysis Date = 07/01/15 Pct Recovery = 92% Analysis Date = 07/01/15 Pct Recovery = 92% Analysis Date = 06/22/15 Pct Recovery = 92% Analysis Date = 06/22/15 Pct Recovery = 92% Analysis Date = 06/12/15 Pct Recovery = 92% Analysis Date = 06/12/15 Pct Recovery = 92% Analysis Date = 06/03/15 Pct Recovery = 92% Analysis Date = 06/03/15 Pct Recovery = 92% Analysis Date = 05/25/15 Pct Recovery = 92% Analysis Date = 05/25/15 Pct Recovery = 92% Analysis Date = 05/16/15 Pct Recovery = 92% Analysis Date = 05/16/15 Pct Recovery = 92% Analysis Date = 05/06/15 Pct Recovery = 91% Analysis Date = 05/06/15 Pct Recovery = 91% Analysis Date = 04/27/15 Pct Recovery = 91% Analysis Date = 04/27/15 Pct Recovery = 91% Analysis Date = 04/18/15 Pct Recovery = 91% Analysis Date = 04/18/15 Pct Recovery = 91% Analysis Date = 04/09/15 Pct Recovery = 91% Analysis Date = 04/09/15 Pct Recovery = 91% Analysis Date = 03/30/15 Pct Recovery = 91% Analysis Date = 03/30/15 Pct Recovery = 91% Analysis Date = 03/21/15 Pct Recovery = 91% Analysis Date = 03/21/15 Pct Recovery = 91% Analysis Date = 03/12/15 Pct Recovery = 91% Analysis Date = 03/12/15 Pct Recovery = 91% Analysis Date = 03/03/15 Pct Recovery = 91% Analysis Date = 03/03/15 Pct Recovery = 91% Analysis Date = 02/21/15 Pct Recovery = 91% Analysis Date = 02/21/15 Pct Recovery = 91% Analysis Date = 02/12/15 Pct Recovery = 91% Analysis Date = 02/12/15 Pct Recovery = 91% Analysis Date = 02/03/15 Pct Recovery = 91% Analysis Date = 02/03/15 Pct Recovery = 91% Analysis Date = 01/25/15 Pct Recovery = 91% Analysis Date = 01/25/15 Pct Recovery = 91% Analysis Date = 01/15/15 Pct Recovery = 91% Analysis Date = 01/15/15 Pct Recovery = 91% Analysis Date = 01/06/15 Pct Recovery = 91% Analysis Date = 01/06/15 Pct Recovery = 91% Analysis Date = 12/28/14 Pct Recovery = 91% Analysis Date = 12/28/14 Pct Recovery = 91% Analysis Date = 12/19/14 Pct Recovery = 91% Analysis Date = 12/19/14 Pct Recovery = 91% Analysis Date = 12/09/14 Pct Recovery = 91% Analysis Date = 12/09/14 Pct Recovery = 91% Analysis Date = 11/30/14 Pct Recovery = 91% Analysis Date = 11/30/14 Pct Recovery = 91% Analysis Date = 11/21/14 Pct Recovery = 91% Analysis Date = 11/21/14 Pct Recovery = 91% Analysis Date = 11/12/14 Pct Recovery = 91% Analysis Date = 11/12/14 Pct Recovery = 91% Analysis Date = 11/02/14 Pct Recovery = 91% Analysis Date = 11/02/14 Pct Recovery = 91% Analysis Date = 10/24/14 Pct Recovery = 91% Analysis Date = 10/24/14 Pct Recovery = 91% Analysis Date = 10/15/14 Pct Recovery = 91% Analysis Date = 10/15/14 Pct Recovery = 91% Analysis Date = 10/06/14 Pct Recovery = 91% Analysis Date = 10/06/14 Pct Recovery = 91% Analysis Date = 09/26/14 Pct Recovery = 91% Analysis Date = 09/26/14 Pct Recovery = 91% Analysis Date = 09/17/14 Pct Recovery = 91% Analysis Date = 09/17/14 Pct Recovery = 91% Analysis Date = 09/08/14 Pct Recovery = 91% Analysis Date = 09/08/14 Pct Recovery = 91% Analysis Date = 08/30/14 Pct Recovery = 91% Analysis Date = 08/30/14 Pct Recovery = 91% Analysis Date = 08/20/14 Pct Recovery = 91% Analysis Date = 08/20/14 Pct Recovery = 91% Analysis Date = 08/11/14 Pct Recovery = 91% Analysis Date = 08/11/14 Pct Recovery = 91% Analysis Date = 08/02/14 Pct Recovery = 91% Analysis Date = 08/02/14 Pct Recovery = 91% Analysis Date = 07/24/14 Pct Recovery = 91% Analysis Date = 07/24/14 Pct Recovery = 91% Analysis Date = 07/14/14 Pct Recovery = 91% Analysis Date = 07/14/14 Pct Recovery = 91% Analysis Date = 07/05/14 Pct Recovery = 91% Analysis Date = 07/05/14 Pct Recovery = 91% Analysis Date = 06/26/14 Pct Recovery = 91% Analysis Date = 06/26/14 Pct Recovery = 91% Analysis Date = 06/17/14 Pct Recovery = 91% Analysis Date = 06/17/14 Pct Recovery = 91% Analysis Date = 06/07/14 Pct Recovery = 91% Analysis Date = 06/07/14 Pct Recovery = 91% Analysis Date = 05/29/14 Pct Recovery = 91% Analysis Date = 05/29/14 Pct Recovery = 91% Analysis Date = 05/20/14 Pct Recovery = 91% Analysis Date = 05/20/14 Pct Recovery = 91% Analysis Date = 05/11/14 Pct Recovery = 91% Analysis Date = 05/11/14 Pct Recovery = 91% Analysis Date = 05/01/14 Pct Recovery = 91% Analysis Date = 05/01/14 Pct Recovery = 91% Analysis Date = 04/22/14 Pct Recovery = 91% Analysis Date = 04/22/14 Pct Recovery = 91% Analysis Date = 04/13/14 Pct Recovery = 91% Analysis Date = 04/13/14 Pct Recovery = 91% Analysis Date = 04/04/14 Pct Recovery = 91% Analysis Date = 04/04/14 Pct Recovery = 91% Analysis Date = 03/25/14 Pct Recovery = 91% Analysis Date = 03/25/14 Pct Recovery = 91% Analysis Date = 03/16/14 Pct Recovery = 91% Analysis Date = 03/16/14 Pct Recovery = 91% Analysis Date = 03/07/14 Pct Recovery = 91% Analysis Date = 03/07/14 Pct Recovery = 91% Analysis Date = 02/26/14 Pct Recovery = 91% Analysis Date = 02/26/14 Pct Recovery = 91% Analysis Date = 02/16/14 Pct Recovery = 91% Analysis Date = 02/16/14 Pct Recovery = 91% Analysis Date = 02/07/14 Pct Recovery = 91% Analysis Date = 02/07/14 Pct Recovery = 91% Analysis Date = 01/29/14 Pct Recovery = 91% Analysis Date = 01/29/14 Pct Recovery = 91% Analysis Date = 01/20/14 Pct Recovery = 91% Analysis Date = 01/20/14 Pct Recovery = 91% Analysis Date = 01/10/14 Pct Recovery = 91% Analysis Date = 01/10/14 Pct Recovery = 91% Analysis Date = 01/01/14 Pct Recovery = 91% Analysis Date = 01/01/14 Pct Recovery = 91% Analysis Date = 12/23/13 Pct Recovery = 91% Analysis Date = 12/23/13 Pct Recovery = 91% Analysis Date = 12/14/13 Pct Recovery = 91% Analysis Date = 12/14/13 Pct Recovery = 91% Analysis Date = 12/04/13 Pct Recovery = 91% Analysis Date = 12/04/13 Pct Recovery = 91% Analysis Date = 11/25/13 Pct Recovery = 91% Analysis Date = 11/25/13 Pct Recovery = 91% Analysis Date = 11/16/13 Pct Recovery = 91% Analysis Date = 11/16/13 Pct Recovery = 91% Analysis Date = 11/07/13 Pct Recovery = 91% Analysis Date = 11/07/13 Pct Recovery = 91% Analysis Date = 10/28/13 Pct Recovery = 92% Analysis Date = 10/28/13 Pct Recovery = 92% Analysis Date = 10/19/13 Pct Recovery = 92% Analysis Date = 10/19/13 Pct Recovery = 92% Analysis Date = 10/10/13 Pct Recovery = 92% Analysis Date = 10/10/13 Pct Recovery = 92% Analysis Date = 10/01/13 Pct Recovery = 92% Analysis Date = 10/01/13 Pct Recovery = 92% Analysis Date = 09/21/13 Pct Recovery = 92% Analysis Date = 09/21/13 Pct Recovery = 92% Analysis Date = 09/12/13 Pct Recovery = 92% Analysis Date = 09/12/13 Pct Recovery = 92% Analysis Date = 09/03/13 Pct Recovery = 92% Analysis Date = 09/03/13 Pct Recovery = 92% Analysis Date = 08/25/13 Pct Recovery = 92% Analysis Date = 08/25/13 Pct Recovery = 92% Analysis Date = 08/15/13 Pct Recovery = 92% Analysis Date = 08/15/13 Pct Recovery = 92% Analysis Date = 08/06/13 Pct Recovery = 92% Analysis Date = 08/06/13 Pct Recovery = 92% Analysis Date = 07/28/13 Pct Recovery = 92% Analysis Date = 07/28/13 Pct Recovery = 92% Analysis Date = 07/19/13 Pct Recovery = 92% Analysis Date = 07/19/13 Pct Recovery = 92% Analysis Date = 07/09/13 Pct Recovery = 92% Analysis Date = 07/09/13 Pct Recovery = 92% Analysis Date = 06/30/13 Pct Recovery = 92% Analysis Date = 06/30/13 Pct Recovery = 92% Analysis Date = 06/21/13 Pct Recovery = 92% Analysis Date = 06/21/13 Pct Recovery = 92% Analysis Date = 06/12/13 Pct Recovery = 92% Analysis Date = 06/12/13 Pct Recovery = 92% Analysis Date = 06/02/13 Pct Recovery = 92% Analysis Date = 06/02/13 Pct Recovery = 92% Analysis Date = 05/24/13 Pct Recovery = 92% Analysis Date = 05/24/13 Pct Recovery = 92% Analysis Date = 05/15/13 Pct Recovery = 92% Analysis Date = 05/15/13 Pct Recovery = 92% Analysis Date = 05/06/13 Pct Recovery = 92% Analysis Date = 05/06/13 Pct Recovery = 92% Analysis Date = 04/26/13 Pct Recovery = 92% Analysis Date = 04/26/13 Pct Recovery = 92% Analysis Date = 04/17/13 Pct Recovery = 92% Analysis Date = 04/17/13 Pct Recovery = 92% Analysis Date = 04/08/13 Pct Recovery = 92% Analysis Date = 04/08/13 Pct Recovery = 92% Analysis Date = 03/30/13 Pct Recovery = 92% Analysis Date = 03/30/13 Pct Recovery = 92% Analysis Date = 03/20/13 Pct Recovery = 92% Analysis Date = 03/20/13 Pct Recovery = 92% Analysis Date = 03/11/13 Pct Recovery = 92% Analysis Date = 03/11/13 Pct Recovery = 92% Analysis Date = 03/02/13 Pct Recovery = 92% Analysis Date = 03/02/13 Pct Recovery = 92% Analysis Date = 02/21/13 Pct Recovery = 93% Analysis Date = 02/21/13 Pct Recovery = 93% Analysis Date = 02/11/13 Pct Recovery = 93% Analysis Date = 02/11/13 Pct Recovery = 93% Analysis Date = 02/02/13 Pct Recovery = 93% Analysis Date = 02/02/13 Pct Recovery = 93% Analysis Date = 01/24/13 Pct Recovery = 93% Analysis Date = 01/24/13 Pct Recovery = 93% Analysis Date = 01/15/13 Pct Recovery = 93% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
FIPRONIL SULFIDE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 71 91% 12% 91% 11%
Total 71 91% 12% 91% 11%

Sample Statistics
FIPRONIL SULFIDE

Characteristic N % % Basis
Plotted 71 100% Spiked
Estimated Values 1 1% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 71 .  
False Negatives 0 0% 0 out of 71
Not Spiked 47 .  
False Positives 3 6% 3 out of 47

OBSP Determination:
FIPRONIL SULFONE
METHOD: 2033 , TESTIDCODE: 62168GCM29

Laboratory ID = 20132490342 Lab Value = 0.219 Expected Conc. = 0.298 Report level label = 0.024 Pct Recovery = 73% Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20172510330 Lab Value = 0.121 Expected Conc. = 0.16 Report level label = 0.024 Pct Recovery = 76% Analysis Date = 12/29/17 SpikeMix = ChemService 6537100: 100 µl & Abs 071817Pest: 100 µl SpecificMix = 071817Pest Laboratory ID = 20163370001 Lab Value = 0.124 Expected Conc. = 0.151 Report level label = 0.024 Pct Recovery = 82% Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl SpecificMix = B20160331 Laboratory ID = 20163150006 Lab Value = 0.143 Expected Conc. = 0.151 Report level label = 0.024 Pct Recovery = 95% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl SpecificMix = B20160331 Laboratory ID = 20132140002 Lab Value = 0.110 Expected Conc. = 0.15 Report level label = 0.024 Pct Recovery = 73% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl SpecificMix = LB99392 Laboratory ID = 20131370001 Lab Value = 0.254 Expected Conc. = 0.15 Report level label = 0.024 Pct Recovery = 169% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl SpecificMix = LB99392 Laboratory ID = 20161880109 Lab Value = 0.138 Expected Conc. = 0.149 Report level label = 0.024 Pct Recovery = 93% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl SpecificMix = 03FF076 Laboratory ID = 20140370077 Lab Value = 0.094 Expected Conc. = 0.149 Report level label = 0.024 Pct Recovery = 63% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20132560001 Lab Value = 0.111 Expected Conc. = 0.149 Report level label = 0.024 Pct Recovery = 74% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20152610011 Lab Value = 0.100 Expected Conc. = 0.1432 Report level label = 0.024 Pct Recovery = 69% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl SpecificMix = 0406-15-01 Laboratory ID = 20152460215 Lab Value = 0.111 Expected Conc. = 0.1432 Report level label = 0.024 Pct Recovery = 78% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl SpecificMix = 0406-15-01 Laboratory ID = 20171720140 Lab Value = 0.091 Expected Conc. = 0.1208 Report level label = 0.024 Pct Recovery = 75% Analysis Date = 08/31/17 SpikeMix = Supelco LC20138V: 80 µl & Phenova B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20171660002 Lab Value = 0.099 Expected Conc. = 0.1208 Report level label = 0.024 Pct Recovery = 82% Analysis Date = 08/23/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20170190026 Lab Value = 0.108 Expected Conc. = 0.1208 Report level label = 0.024 Pct Recovery = 89% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20161470001 Lab Value = 0.119 Expected Conc. = 0.1208 Report level label = 0.024 Pct Recovery = 99% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20170960001 Lab Value = 0.089 Expected Conc. = 0.1192 Report level label = 0.024 Pct Recovery = 74% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl SpecificMix = 03FF076 Laboratory ID = 20130940097 Lab Value = 0.081 Expected Conc. = 0.1015 Report level label = 0.024 Pct Recovery = 80% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = 0507-12-04.2 Laboratory ID = 20123560092 Lab Value = 0.079 Expected Conc. = 0.1015 Report level label = 0.024 Pct Recovery = 78% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = 0507-12-04.2 Laboratory ID = 20130810108 Lab Value = 0.088 Expected Conc. = 0.1 Report level label = 0.024 Pct Recovery = 87% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl SpecificMix = LB92783 Laboratory ID = 20130100066 Lab Value = 0.080 Expected Conc. = 0.1 Report level label = 0.024 Pct Recovery = 80% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl SpecificMix = LB92783 Laboratory ID = 20150430092 Lab Value = 0.085 Expected Conc. = 0.096 Report level label = 0.024 Pct Recovery = 88% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl SpecificMix = E1140407002 Laboratory ID = 20143240095 Lab Value = 0.072 Expected Conc. = 0.096 Report level label = 0.024 Pct Recovery = 75% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl SpecificMix = 032714 Laboratory ID = 20143110108 Lab Value = 0.064 Expected Conc. = 0.096 Report level label = 0.024 Pct Recovery = 66% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl SpecificMix = E1140407002 Laboratory ID = 20142720002 Lab Value = 0.079 Expected Conc. = 0.096 Report level label = 0.024 Pct Recovery = 82% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl SpecificMix = E1140407002 Laboratory ID = 20142270001 Lab Value = 0.060 Expected Conc. = 0.096 Report level label = 0.024 Pct Recovery = 62% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl SpecificMix = 032714 Laboratory ID = 20141770149 Lab Value = 0.089 Expected Conc. = 0.096 Report level label = 0.024 Pct Recovery = 93% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl SpecificMix = E1140407002 Laboratory ID = 20141220025 Lab Value = 0.071 Expected Conc. = 0.096 Report level label = 0.024 Pct Recovery = 74% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl SpecificMix = 032714 Laboratory ID = 20172560101 Lab Value = 0.059 Expected Conc. = 0.08 Report level label = 0.024 Pct Recovery = 74% Analysis Date = 12/22/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6567600: 50 µl SpecificMix = 6567600 Laboratory ID = 20161260151 Lab Value = 0.068 Expected Conc. = 0.072 Report level label = 0.024 Pct Recovery = 95% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = 3851600 Laboratory ID = 20151550293 Lab Value = 0.057 Expected Conc. = 0.072 Report level label = 0.024 Pct Recovery = 79% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl SpecificMix = 3851600 Laboratory ID = 20151270112 Lab Value = 0.051 Expected Conc. = 0.072 Report level label = 0.024 Pct Recovery = 71% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl SpecificMix = 3851600 Laboratory ID = 20160770090 Lab Value = 0.061 Expected Conc. = 0.0716 Report level label = 0.024 Pct Recovery = 85% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20160630046 Lab Value = 0.061 Expected Conc. = 0.0716 Report level label = 0.024 Pct Recovery = 85% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20153510109 Lab Value = 0.057 Expected Conc. = 0.0716 Report level label = 0.024 Pct Recovery = 80% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20153440001 Lab Value = 0.063 Expected Conc. = 0.0716 Report level label = 0.024 Pct Recovery = 88% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20171160110 Lab Value = 0.056 Expected Conc. = 0.0604 Report level label = 0.024 Pct Recovery = 93% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = B20160331 Laboratory ID = 20162380004 Lab Value = 0.045 Expected Conc. = 0.0604 Report level label = 0.024 Pct Recovery = 75% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = B20160331 Laboratory ID = 20162150213 Lab Value = 0.056 Expected Conc. = 0.0604 Report level label = 0.024 Pct Recovery = 92% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl SpecificMix = B20160331 Laboratory ID = 20140510043 Lab Value = 0.047 Expected Conc. = 0.06 Report level label = 0.024 Pct Recovery = 79% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl SpecificMix = LB99392 Laboratory ID = 20133470008 Lab Value = 0.052 Expected Conc. = 0.06 Report level label = 0.024 Pct Recovery = 87% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl SpecificMix = LB99392 Laboratory ID = 20133190012 Lab Value = 0.078 Expected Conc. = 0.06 Report level label = 0.024 Pct Recovery = 131% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = LB99392 Laboratory ID = 20133050050 Lab Value = 0.052 Expected Conc. = 0.06 Report level label = 0.024 Pct Recovery = 86% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl SpecificMix = LB99392 Laboratory ID = 20172020035 Lab Value = 0.061 Expected Conc. = 0.0596 Report level label = 0.024 Pct Recovery = 102% Analysis Date = 11/07/17 SpikeMix = Abs 071717Pest: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20171510080 Lab Value = 0.058 Expected Conc. = 0.0596 Report level label = 0.024 Pct Recovery = 98% Analysis Date = 06/09/17 SpikeMix = Supelco LC20138V: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20170460061 Lab Value = 0.046 Expected Conc. = 0.0596 Report level label = 0.024 Pct Recovery = 78% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl SpecificMix = 03FF076 Laboratory ID = 20162660005 Lab Value = 0.046 Expected Conc. = 0.0596 Report level label = 0.024 Pct Recovery = 78% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl SpecificMix = 03FF076 Laboratory ID = 20161600087 Lab Value = 0.061 Expected Conc. = 0.0596 Report level label = 0.024 Pct Recovery = 103% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20161340228 Lab Value = 0.073 Expected Conc. = 0.0596 Report level label = 0.024 Pct Recovery = 122% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl SpecificMix = 03FF076 Laboratory ID = 20161190075 Lab Value = 0.061 Expected Conc. = 0.0596 Report level label = 0.024 Pct Recovery = 102% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20133580036 Lab Value = 0.043 Expected Conc. = 0.0596 Report level label = 0.024 Pct Recovery = 72% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20131790009 Lab Value = 0.050 Expected Conc. = 0.0596 Report level label = 0.024 Pct Recovery = 84% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20131510026 Lab Value = 0.062 Expected Conc. = 0.0596 Report level label = 0.024 Pct Recovery = 104% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20172780018 Lab Value = 0.044 Expected Conc. = 0.048 Report level label = 0.024 Pct Recovery = 92% Analysis Date = 02/08/18 SpikeMix = ChemService 6537100: 30 µl & Abs 071817Pest: 30 µl SpecificMix = 071817Pest Laboratory ID = 20150150115 Lab Value = 0.043 Expected Conc. = 0.048 Report level label = 0.024 Pct Recovery = 89% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl SpecificMix = 032714 Laboratory ID = 20142820151 Lab Value = 0.052 Expected Conc. = 0.048 Report level label = 0.024 Pct Recovery = 108% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl SpecificMix = 032714 Laboratory ID = 20142470041 Lab Value = 0.047 Expected Conc. = 0.048 Report level label = 0.024 Pct Recovery = 97% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141910243 Lab Value = 0.035 Expected Conc. = 0.048 Report level label = 0.024 Pct Recovery = 72% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141640076 Lab Value = 0.030 Expected Conc. = 0.048 Report level label = 0.024 Pct Recovery = 62% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141490205 Lab Value = 0.051 Expected Conc. = 0.048 Report level label = 0.024 Pct Recovery = 106% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = 032714 Laboratory ID = 20141360094 Lab Value = 0.049 Expected Conc. = 0.048 Report level label = 0.024 Pct Recovery = 102% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141080004 Lab Value = 0.028 Expected Conc. = 0.048 Report level label = 0.024 Pct Recovery = 59% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl SpecificMix = 032714 Laboratory ID = 20130510051 Lab Value = 0.035 Expected Conc. = 0.0406 Report level label = 0.024 Pct Recovery = 86% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl SpecificMix = 0507-12-04.2 Laboratory ID = 20130390105 Lab Value = 0.041 Expected Conc. = 0.04 Report level label = 0.024 Pct Recovery = 101% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl SpecificMix = LB92783 Laboratory ID = 20160430111 Lab Value = 0.037 Expected Conc. = 0.036 Report level label = 0.024 Pct Recovery = 103% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 3851600 Laboratory ID = 20160210080 Lab Value = 0.032 Expected Conc. = 0.036 Report level label = 0.024 Pct Recovery = 89% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 3851600 Laboratory ID = 20152950078 Lab Value = 0.023 Expected Conc. = 0.036 Report level label = 0.024 Pct Recovery = 64% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 3851600 Laboratory ID = 20153030068 Lab Value = 0.036 Expected Conc. = 0.036 Report level label = 0.024 Pct Recovery = 99% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = 3851600 Laboratory ID = 20151760208 Lab Value = 0.039 Expected Conc. = 0.036 Report level label = 0.024 Pct Recovery = 108% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl SpecificMix = 3851600 Laboratory ID = 20151380009 Lab Value = 0.027 Expected Conc. = 0.036 Report level label = 0.024 Pct Recovery = 74% Analysis Date = 05/30/15 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 3851600 Laboratory ID = 20152190003 Lab Value = 0.029 Expected Conc. = 0.0358 Report level label = 0.024 Pct Recovery = 81% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = 0406-15-01 Laboratory ID = 20152040177 Lab Value = 0.033 Expected Conc. = 0.0358 Report level label = 0.024 Pct Recovery = 92% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl SpecificMix = 0406-15-01 Analysis Date = 02/08/18 Pct Recovery = 84% Analysis Date = 01/29/18 Pct Recovery = 84% Analysis Date = 01/29/18 Pct Recovery = 84% Analysis Date = 01/20/18 Pct Recovery = 84% Analysis Date = 01/20/18 Pct Recovery = 84% Analysis Date = 01/11/18 Pct Recovery = 84% Analysis Date = 01/11/18 Pct Recovery = 84% Analysis Date = 01/02/18 Pct Recovery = 84% Analysis Date = 01/02/18 Pct Recovery = 84% Analysis Date = 12/23/17 Pct Recovery = 84% Analysis Date = 12/23/17 Pct Recovery = 84% Analysis Date = 12/14/17 Pct Recovery = 84% Analysis Date = 12/14/17 Pct Recovery = 84% Analysis Date = 12/05/17 Pct Recovery = 85% Analysis Date = 12/05/17 Pct Recovery = 85% Analysis Date = 11/26/17 Pct Recovery = 85% Analysis Date = 11/26/17 Pct Recovery = 85% Analysis Date = 11/16/17 Pct Recovery = 85% Analysis Date = 11/16/17 Pct Recovery = 85% Analysis Date = 11/07/17 Pct Recovery = 85% Analysis Date = 11/07/17 Pct Recovery = 85% Analysis Date = 10/29/17 Pct Recovery = 85% Analysis Date = 10/29/17 Pct Recovery = 85% Analysis Date = 10/20/17 Pct Recovery = 85% Analysis Date = 10/20/17 Pct Recovery = 85% Analysis Date = 10/10/17 Pct Recovery = 85% Analysis Date = 10/10/17 Pct Recovery = 85% Analysis Date = 10/01/17 Pct Recovery = 85% Analysis Date = 10/01/17 Pct Recovery = 85% Analysis Date = 09/22/17 Pct Recovery = 85% Analysis Date = 09/22/17 Pct Recovery = 85% Analysis Date = 09/13/17 Pct Recovery = 85% Analysis Date = 09/13/17 Pct Recovery = 85% Analysis Date = 09/03/17 Pct Recovery = 86% Analysis Date = 09/03/17 Pct Recovery = 86% Analysis Date = 08/25/17 Pct Recovery = 86% Analysis Date = 08/25/17 Pct Recovery = 86% Analysis Date = 08/16/17 Pct Recovery = 86% Analysis Date = 08/16/17 Pct Recovery = 86% Analysis Date = 08/07/17 Pct Recovery = 86% Analysis Date = 08/07/17 Pct Recovery = 86% Analysis Date = 07/28/17 Pct Recovery = 86% Analysis Date = 07/28/17 Pct Recovery = 86% Analysis Date = 07/19/17 Pct Recovery = 86% Analysis Date = 07/19/17 Pct Recovery = 86% Analysis Date = 07/10/17 Pct Recovery = 86% Analysis Date = 07/10/17 Pct Recovery = 86% Analysis Date = 07/01/17 Pct Recovery = 86% Analysis Date = 07/01/17 Pct Recovery = 86% Analysis Date = 06/21/17 Pct Recovery = 86% Analysis Date = 06/21/17 Pct Recovery = 86% Analysis Date = 06/12/17 Pct Recovery = 86% Analysis Date = 06/12/17 Pct Recovery = 86% Analysis Date = 06/03/17 Pct Recovery = 87% Analysis Date = 06/03/17 Pct Recovery = 87% Analysis Date = 05/25/17 Pct Recovery = 87% Analysis Date = 05/25/17 Pct Recovery = 87% Analysis Date = 05/15/17 Pct Recovery = 87% Analysis Date = 05/15/17 Pct Recovery = 87% Analysis Date = 05/06/17 Pct Recovery = 87% Analysis Date = 05/06/17 Pct Recovery = 87% Analysis Date = 04/27/17 Pct Recovery = 87% Analysis Date = 04/27/17 Pct Recovery = 87% Analysis Date = 04/18/17 Pct Recovery = 87% Analysis Date = 04/18/17 Pct Recovery = 87% Analysis Date = 04/08/17 Pct Recovery = 87% Analysis Date = 04/08/17 Pct Recovery = 87% Analysis Date = 03/30/17 Pct Recovery = 87% Analysis Date = 03/30/17 Pct Recovery = 87% Analysis Date = 03/21/17 Pct Recovery = 87% Analysis Date = 03/21/17 Pct Recovery = 87% Analysis Date = 03/12/17 Pct Recovery = 87% Analysis Date = 03/12/17 Pct Recovery = 87% Analysis Date = 03/02/17 Pct Recovery = 87% Analysis Date = 03/02/17 Pct Recovery = 87% Analysis Date = 02/21/17 Pct Recovery = 87% Analysis Date = 02/21/17 Pct Recovery = 87% Analysis Date = 02/12/17 Pct Recovery = 87% Analysis Date = 02/12/17 Pct Recovery = 87% Analysis Date = 02/03/17 Pct Recovery = 88% Analysis Date = 02/03/17 Pct Recovery = 88% Analysis Date = 01/24/17 Pct Recovery = 88% Analysis Date = 01/24/17 Pct Recovery = 88% Analysis Date = 01/15/17 Pct Recovery = 88% Analysis Date = 01/15/17 Pct Recovery = 88% Analysis Date = 01/06/17 Pct Recovery = 88% Analysis Date = 01/06/17 Pct Recovery = 88% Analysis Date = 12/28/16 Pct Recovery = 88% Analysis Date = 12/28/16 Pct Recovery = 88% Analysis Date = 12/18/16 Pct Recovery = 88% Analysis Date = 12/18/16 Pct Recovery = 88% Analysis Date = 12/09/16 Pct Recovery = 88% Analysis Date = 12/09/16 Pct Recovery = 88% Analysis Date = 11/30/16 Pct Recovery = 88% Analysis Date = 11/30/16 Pct Recovery = 88% Analysis Date = 11/21/16 Pct Recovery = 88% Analysis Date = 11/21/16 Pct Recovery = 88% Analysis Date = 11/11/16 Pct Recovery = 88% Analysis Date = 11/11/16 Pct Recovery = 88% Analysis Date = 11/02/16 Pct Recovery = 88% Analysis Date = 11/02/16 Pct Recovery = 88% Analysis Date = 10/24/16 Pct Recovery = 88% Analysis Date = 10/24/16 Pct Recovery = 88% Analysis Date = 10/15/16 Pct Recovery = 88% Analysis Date = 10/15/16 Pct Recovery = 88% Analysis Date = 10/05/16 Pct Recovery = 88% Analysis Date = 10/05/16 Pct Recovery = 88% Analysis Date = 09/26/16 Pct Recovery = 88% Analysis Date = 09/26/16 Pct Recovery = 88% Analysis Date = 09/17/16 Pct Recovery = 88% Analysis Date = 09/17/16 Pct Recovery = 88% Analysis Date = 09/08/16 Pct Recovery = 88% Analysis Date = 09/08/16 Pct Recovery = 88% Analysis Date = 08/29/16 Pct Recovery = 88% Analysis Date = 08/29/16 Pct Recovery = 88% Analysis Date = 08/20/16 Pct Recovery = 89% Analysis Date = 08/20/16 Pct Recovery = 89% Analysis Date = 08/11/16 Pct Recovery = 89% Analysis Date = 08/11/16 Pct Recovery = 89% Analysis Date = 08/02/16 Pct Recovery = 89% Analysis Date = 08/02/16 Pct Recovery = 89% Analysis Date = 07/23/16 Pct Recovery = 89% Analysis Date = 07/23/16 Pct Recovery = 89% Analysis Date = 07/14/16 Pct Recovery = 89% Analysis Date = 07/14/16 Pct Recovery = 89% Analysis Date = 07/05/16 Pct Recovery = 89% Analysis Date = 07/05/16 Pct Recovery = 89% Analysis Date = 06/26/16 Pct Recovery = 89% Analysis Date = 06/26/16 Pct Recovery = 89% Analysis Date = 06/16/16 Pct Recovery = 89% Analysis Date = 06/16/16 Pct Recovery = 89% Analysis Date = 06/07/16 Pct Recovery = 89% Analysis Date = 06/07/16 Pct Recovery = 89% Analysis Date = 05/29/16 Pct Recovery = 89% Analysis Date = 05/29/16 Pct Recovery = 89% Analysis Date = 05/20/16 Pct Recovery = 89% Analysis Date = 05/20/16 Pct Recovery = 89% Analysis Date = 05/10/16 Pct Recovery = 89% Analysis Date = 05/10/16 Pct Recovery = 89% Analysis Date = 05/01/16 Pct Recovery = 89% Analysis Date = 05/01/16 Pct Recovery = 89% Analysis Date = 04/22/16 Pct Recovery = 89% Analysis Date = 04/22/16 Pct Recovery = 89% Analysis Date = 04/13/16 Pct Recovery = 89% Analysis Date = 04/13/16 Pct Recovery = 89% Analysis Date = 04/03/16 Pct Recovery = 88% Analysis Date = 04/03/16 Pct Recovery = 88% Analysis Date = 03/25/16 Pct Recovery = 88% Analysis Date = 03/25/16 Pct Recovery = 88% Analysis Date = 03/16/16 Pct Recovery = 88% Analysis Date = 03/16/16 Pct Recovery = 88% Analysis Date = 03/07/16 Pct Recovery = 88% Analysis Date = 03/07/16 Pct Recovery = 88% Analysis Date = 02/26/16 Pct Recovery = 88% Analysis Date = 02/26/16 Pct Recovery = 88% Analysis Date = 02/17/16 Pct Recovery = 88% Analysis Date = 02/17/16 Pct Recovery = 88% Analysis Date = 02/08/16 Pct Recovery = 88% Analysis Date = 02/08/16 Pct Recovery = 88% Analysis Date = 01/30/16 Pct Recovery = 88% Analysis Date = 01/30/16 Pct Recovery = 88% Analysis Date = 01/20/16 Pct Recovery = 88% Analysis Date = 01/20/16 Pct Recovery = 88% Analysis Date = 01/11/16 Pct Recovery = 88% Analysis Date = 01/11/16 Pct Recovery = 88% Analysis Date = 01/02/16 Pct Recovery = 88% Analysis Date = 01/02/16 Pct Recovery = 88% Analysis Date = 12/24/15 Pct Recovery = 88% Analysis Date = 12/24/15 Pct Recovery = 88% Analysis Date = 12/14/15 Pct Recovery = 87% Analysis Date = 12/14/15 Pct Recovery = 87% Analysis Date = 12/05/15 Pct Recovery = 87% Analysis Date = 12/05/15 Pct Recovery = 87% Analysis Date = 11/26/15 Pct Recovery = 87% Analysis Date = 11/26/15 Pct Recovery = 87% Analysis Date = 11/17/15 Pct Recovery = 87% Analysis Date = 11/17/15 Pct Recovery = 87% Analysis Date = 11/07/15 Pct Recovery = 87% Analysis Date = 11/07/15 Pct Recovery = 87% Analysis Date = 10/29/15 Pct Recovery = 87% Analysis Date = 10/29/15 Pct Recovery = 87% Analysis Date = 10/20/15 Pct Recovery = 87% Analysis Date = 10/20/15 Pct Recovery = 87% Analysis Date = 10/11/15 Pct Recovery = 86% Analysis Date = 10/11/15 Pct Recovery = 86% Analysis Date = 10/01/15 Pct Recovery = 86% Analysis Date = 10/01/15 Pct Recovery = 86% Analysis Date = 09/22/15 Pct Recovery = 86% Analysis Date = 09/22/15 Pct Recovery = 86% Analysis Date = 09/13/15 Pct Recovery = 86% Analysis Date = 09/13/15 Pct Recovery = 86% Analysis Date = 09/04/15 Pct Recovery = 86% Analysis Date = 09/04/15 Pct Recovery = 86% Analysis Date = 08/25/15 Pct Recovery = 86% Analysis Date = 08/25/15 Pct Recovery = 86% Analysis Date = 08/16/15 Pct Recovery = 86% Analysis Date = 08/16/15 Pct Recovery = 86% Analysis Date = 08/07/15 Pct Recovery = 85% Analysis Date = 08/07/15 Pct Recovery = 85% Analysis Date = 07/29/15 Pct Recovery = 85% Analysis Date = 07/29/15 Pct Recovery = 85% Analysis Date = 07/19/15 Pct Recovery = 85% Analysis Date = 07/19/15 Pct Recovery = 85% Analysis Date = 07/10/15 Pct Recovery = 85% Analysis Date = 07/10/15 Pct Recovery = 85% Analysis Date = 07/01/15 Pct Recovery = 85% Analysis Date = 07/01/15 Pct Recovery = 85% Analysis Date = 06/22/15 Pct Recovery = 85% Analysis Date = 06/22/15 Pct Recovery = 85% Analysis Date = 06/12/15 Pct Recovery = 84% Analysis Date = 06/12/15 Pct Recovery = 84% Analysis Date = 06/03/15 Pct Recovery = 84% Analysis Date = 06/03/15 Pct Recovery = 84% Analysis Date = 05/25/15 Pct Recovery = 84% Analysis Date = 05/25/15 Pct Recovery = 84% Analysis Date = 05/16/15 Pct Recovery = 84% Analysis Date = 05/16/15 Pct Recovery = 84% Analysis Date = 05/06/15 Pct Recovery = 84% Analysis Date = 05/06/15 Pct Recovery = 84% Analysis Date = 04/27/15 Pct Recovery = 84% Analysis Date = 04/27/15 Pct Recovery = 84% Analysis Date = 04/18/15 Pct Recovery = 84% Analysis Date = 04/18/15 Pct Recovery = 84% Analysis Date = 04/09/15 Pct Recovery = 83% Analysis Date = 04/09/15 Pct Recovery = 83% Analysis Date = 03/30/15 Pct Recovery = 83% Analysis Date = 03/30/15 Pct Recovery = 83% Analysis Date = 03/21/15 Pct Recovery = 83% Analysis Date = 03/21/15 Pct Recovery = 83% Analysis Date = 03/12/15 Pct Recovery = 83% Analysis Date = 03/12/15 Pct Recovery = 83% Analysis Date = 03/03/15 Pct Recovery = 83% Analysis Date = 03/03/15 Pct Recovery = 83% Analysis Date = 02/21/15 Pct Recovery = 83% Analysis Date = 02/21/15 Pct Recovery = 83% Analysis Date = 02/12/15 Pct Recovery = 83% Analysis Date = 02/12/15 Pct Recovery = 83% Analysis Date = 02/03/15 Pct Recovery = 82% Analysis Date = 02/03/15 Pct Recovery = 82% Analysis Date = 01/25/15 Pct Recovery = 82% Analysis Date = 01/25/15 Pct Recovery = 82% Analysis Date = 01/15/15 Pct Recovery = 82% Analysis Date = 01/15/15 Pct Recovery = 82% Analysis Date = 01/06/15 Pct Recovery = 82% Analysis Date = 01/06/15 Pct Recovery = 82% Analysis Date = 12/28/14 Pct Recovery = 82% Analysis Date = 12/28/14 Pct Recovery = 82% Analysis Date = 12/19/14 Pct Recovery = 82% Analysis Date = 12/19/14 Pct Recovery = 82% Analysis Date = 12/09/14 Pct Recovery = 82% Analysis Date = 12/09/14 Pct Recovery = 82% Analysis Date = 11/30/14 Pct Recovery = 82% Analysis Date = 11/30/14 Pct Recovery = 82% Analysis Date = 11/21/14 Pct Recovery = 82% Analysis Date = 11/21/14 Pct Recovery = 82% Analysis Date = 11/12/14 Pct Recovery = 82% Analysis Date = 11/12/14 Pct Recovery = 82% Analysis Date = 11/02/14 Pct Recovery = 82% Analysis Date = 11/02/14 Pct Recovery = 82% Analysis Date = 10/24/14 Pct Recovery = 82% Analysis Date = 10/24/14 Pct Recovery = 82% Analysis Date = 10/15/14 Pct Recovery = 82% Analysis Date = 10/15/14 Pct Recovery = 82% Analysis Date = 10/06/14 Pct Recovery = 82% Analysis Date = 10/06/14 Pct Recovery = 82% Analysis Date = 09/26/14 Pct Recovery = 82% Analysis Date = 09/26/14 Pct Recovery = 82% Analysis Date = 09/17/14 Pct Recovery = 82% Analysis Date = 09/17/14 Pct Recovery = 82% Analysis Date = 09/08/14 Pct Recovery = 83% Analysis Date = 09/08/14 Pct Recovery = 83% Analysis Date = 08/30/14 Pct Recovery = 83% Analysis Date = 08/30/14 Pct Recovery = 83% Analysis Date = 08/20/14 Pct Recovery = 83% Analysis Date = 08/20/14 Pct Recovery = 83% Analysis Date = 08/11/14 Pct Recovery = 83% Analysis Date = 08/11/14 Pct Recovery = 83% Analysis Date = 08/02/14 Pct Recovery = 83% Analysis Date = 08/02/14 Pct Recovery = 83% Analysis Date = 07/24/14 Pct Recovery = 83% Analysis Date = 07/24/14 Pct Recovery = 83% Analysis Date = 07/14/14 Pct Recovery = 83% Analysis Date = 07/14/14 Pct Recovery = 83% Analysis Date = 07/05/14 Pct Recovery = 83% Analysis Date = 07/05/14 Pct Recovery = 83% Analysis Date = 06/26/14 Pct Recovery = 84% Analysis Date = 06/26/14 Pct Recovery = 84% Analysis Date = 06/17/14 Pct Recovery = 84% Analysis Date = 06/17/14 Pct Recovery = 84% Analysis Date = 06/07/14 Pct Recovery = 84% Analysis Date = 06/07/14 Pct Recovery = 84% Analysis Date = 05/29/14 Pct Recovery = 84% Analysis Date = 05/29/14 Pct Recovery = 84% Analysis Date = 05/20/14 Pct Recovery = 84% Analysis Date = 05/20/14 Pct Recovery = 84% Analysis Date = 05/11/14 Pct Recovery = 84% Analysis Date = 05/11/14 Pct Recovery = 84% Analysis Date = 05/01/14 Pct Recovery = 85% Analysis Date = 05/01/14 Pct Recovery = 85% Analysis Date = 04/22/14 Pct Recovery = 85% Analysis Date = 04/22/14 Pct Recovery = 85% Analysis Date = 04/13/14 Pct Recovery = 85% Analysis Date = 04/13/14 Pct Recovery = 85% Analysis Date = 04/04/14 Pct Recovery = 85% Analysis Date = 04/04/14 Pct Recovery = 85% Analysis Date = 03/25/14 Pct Recovery = 85% Analysis Date = 03/25/14 Pct Recovery = 85% Analysis Date = 03/16/14 Pct Recovery = 86% Analysis Date = 03/16/14 Pct Recovery = 86% Analysis Date = 03/07/14 Pct Recovery = 86% Analysis Date = 03/07/14 Pct Recovery = 86% Analysis Date = 02/26/14 Pct Recovery = 86% Analysis Date = 02/26/14 Pct Recovery = 86% Analysis Date = 02/16/14 Pct Recovery = 86% Analysis Date = 02/16/14 Pct Recovery = 86% Analysis Date = 02/07/14 Pct Recovery = 86% Analysis Date = 02/07/14 Pct Recovery = 86% Analysis Date = 01/29/14 Pct Recovery = 86% Analysis Date = 01/29/14 Pct Recovery = 86% Analysis Date = 01/20/14 Pct Recovery = 86% Analysis Date = 01/20/14 Pct Recovery = 86% Analysis Date = 01/10/14 Pct Recovery = 87% Analysis Date = 01/10/14 Pct Recovery = 87% Analysis Date = 01/01/14 Pct Recovery = 87% Analysis Date = 01/01/14 Pct Recovery = 87% Analysis Date = 12/23/13 Pct Recovery = 87% Analysis Date = 12/23/13 Pct Recovery = 87% Analysis Date = 12/14/13 Pct Recovery = 87% Analysis Date = 12/14/13 Pct Recovery = 87% Analysis Date = 12/04/13 Pct Recovery = 87% Analysis Date = 12/04/13 Pct Recovery = 87% Analysis Date = 11/25/13 Pct Recovery = 87% Analysis Date = 11/25/13 Pct Recovery = 87% Analysis Date = 11/16/13 Pct Recovery = 88% Analysis Date = 11/16/13 Pct Recovery = 88% Analysis Date = 11/07/13 Pct Recovery = 88% Analysis Date = 11/07/13 Pct Recovery = 88% Analysis Date = 10/28/13 Pct Recovery = 88% Analysis Date = 10/28/13 Pct Recovery = 88% Analysis Date = 10/19/13 Pct Recovery = 88% Analysis Date = 10/19/13 Pct Recovery = 88% Analysis Date = 10/10/13 Pct Recovery = 88% Analysis Date = 10/10/13 Pct Recovery = 88% Analysis Date = 10/01/13 Pct Recovery = 88% Analysis Date = 10/01/13 Pct Recovery = 88% Analysis Date = 09/21/13 Pct Recovery = 88% Analysis Date = 09/21/13 Pct Recovery = 88% Analysis Date = 09/12/13 Pct Recovery = 89% Analysis Date = 09/12/13 Pct Recovery = 89% Analysis Date = 09/03/13 Pct Recovery = 89% Analysis Date = 09/03/13 Pct Recovery = 89% Analysis Date = 08/25/13 Pct Recovery = 89% Analysis Date = 08/25/13 Pct Recovery = 89% Analysis Date = 08/15/13 Pct Recovery = 89% Analysis Date = 08/15/13 Pct Recovery = 89% Analysis Date = 08/06/13 Pct Recovery = 89% Analysis Date = 08/06/13 Pct Recovery = 89% Analysis Date = 07/28/13 Pct Recovery = 89% Analysis Date = 07/28/13 Pct Recovery = 89% Analysis Date = 07/19/13 Pct Recovery = 90% Analysis Date = 07/19/13 Pct Recovery = 90% Analysis Date = 07/09/13 Pct Recovery = 90% Analysis Date = 07/09/13 Pct Recovery = 90% Analysis Date = 06/30/13 Pct Recovery = 90% Analysis Date = 06/30/13 Pct Recovery = 90% Analysis Date = 06/21/13 Pct Recovery = 90% Analysis Date = 06/21/13 Pct Recovery = 90% Analysis Date = 06/12/13 Pct Recovery = 90% Analysis Date = 06/12/13 Pct Recovery = 90% Analysis Date = 06/02/13 Pct Recovery = 90% Analysis Date = 06/02/13 Pct Recovery = 90% Analysis Date = 05/24/13 Pct Recovery = 91% Analysis Date = 05/24/13 Pct Recovery = 91% Analysis Date = 05/15/13 Pct Recovery = 91% Analysis Date = 05/15/13 Pct Recovery = 91% Analysis Date = 05/06/13 Pct Recovery = 91% Analysis Date = 05/06/13 Pct Recovery = 91% Analysis Date = 04/26/13 Pct Recovery = 91% Analysis Date = 04/26/13 Pct Recovery = 91% Analysis Date = 04/17/13 Pct Recovery = 91% Analysis Date = 04/17/13 Pct Recovery = 91% Analysis Date = 04/08/13 Pct Recovery = 91% Analysis Date = 04/08/13 Pct Recovery = 91% Analysis Date = 03/30/13 Pct Recovery = 92% Analysis Date = 03/30/13 Pct Recovery = 92% Analysis Date = 03/20/13 Pct Recovery = 92% Analysis Date = 03/20/13 Pct Recovery = 92% Analysis Date = 03/11/13 Pct Recovery = 92% Analysis Date = 03/11/13 Pct Recovery = 92% Analysis Date = 03/02/13 Pct Recovery = 92% Analysis Date = 03/02/13 Pct Recovery = 92% Analysis Date = 02/21/13 Pct Recovery = 92% Analysis Date = 02/21/13 Pct Recovery = 92% Analysis Date = 02/11/13 Pct Recovery = 93% Analysis Date = 02/11/13 Pct Recovery = 93% Analysis Date = 02/02/13 Pct Recovery = 93% Analysis Date = 02/02/13 Pct Recovery = 93% Analysis Date = 01/24/13 Pct Recovery = 93% Analysis Date = 01/24/13 Pct Recovery = 93% Analysis Date = 01/15/13 Pct Recovery = 93% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
FIPRONIL SULFONE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 71 87% 17% 85% 15%
Total 71 87% 17% 85% 15%

Sample Statistics
FIPRONIL SULFONE

Characteristic N % % Basis
Plotted 71 100% Spiked
Estimated Values 4 6% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 71 .  
False Negatives 0 0% 0 out of 71
Not Spiked 43 .  
False Positives 2 5% 2 out of 43

OBSP Determination:
FONOFOS
METHOD: 2033 , TESTIDCODE: 04095GCM35

Laboratory ID = 20130250061 Lab Value = 0.463 Expected Conc. = 0.5 Report level label = 0.0048 Pct Recovery = 93% Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl SpecificMix = A088380 Laboratory ID = 20140230082 Lab Value = 0.224 Expected Conc. = 0.25 Report level label = 0.0048 Pct Recovery = 90% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl SpecificMix = A093651 Laboratory ID = 20132420001 Lab Value = 0.220 Expected Conc. = 0.25 Report level label = 0.0048 Pct Recovery = 88% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl SpecificMix = A093651 Laboratory ID = 20130810108 Lab Value = 0.276 Expected Conc. = 0.2495 Report level label = 0.0048 Pct Recovery = 111% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl SpecificMix = T1120530013 Laboratory ID = 20123560092 Lab Value = 0.311 Expected Conc. = 0.2495 Report level label = 0.0048 Pct Recovery = 125% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = T1120530013 Laboratory ID = 20140860102 Lab Value = 0.069 Expected Conc. = 0.1 Report level label = 0.0048 Pct Recovery = 69% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl SpecificMix = A093651 Laboratory ID = 20133400002 Lab Value = 0.093 Expected Conc. = 0.1 Report level label = 0.0048 Pct Recovery = 93% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = A093651 Laboratory ID = 20132910008 Lab Value = 0.085 Expected Conc. = 0.1 Report level label = 0.0048 Pct Recovery = 85% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = A093651 Laboratory ID = 20131920149 Lab Value = 0.090 Expected Conc. = 0.1 Report level label = 0.0048 Pct Recovery = 90% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl SpecificMix = A093651 Laboratory ID = 20131230084 Lab Value = 0.080 Expected Conc. = 0.1 Report level label = 0.0048 Pct Recovery = 80% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl SpecificMix = A088380 Laboratory ID = 20130650005 Lab Value = 0.063 Expected Conc. = 0.1 Report level label = 0.0048 Pct Recovery = 63% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl SpecificMix = A088380 Laboratory ID = 20130390105 Lab Value = 0.088 Expected Conc. = 0.0998 Report level label = 0.0048 Pct Recovery = 89% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl SpecificMix = T1120530013 Laboratory ID = 20180390003 Lab Value = 0.029 Expected Conc. = 0.032 Report level label = 0.008 Pct Recovery = 92% Analysis Date = 04/06/18 SpikeMix = Spex Organics EN170808006: 100 µl & Abs 071717Pest: 100 µl SpecificMix = 071717Pest Laboratory ID = 20172510330 Lab Value = 0.029 Expected Conc. = 0.032 Report level label = 0.0048 Pct Recovery = 89% Analysis Date = 12/29/17 SpikeMix = ChemService 6537100: 100 µl & Abs 071817Pest: 100 µl SpecificMix = 6537100 Laboratory ID = 20162860079 Lab Value = 0.029 Expected Conc. = 0.03 Report level label = 0.0048 Pct Recovery = 98% Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl SpecificMix = 060916 Laboratory ID = 20163150006 Lab Value = 0.032 Expected Conc. = 0.03 Report level label = 0.0048 Pct Recovery = 108% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl SpecificMix = 060916 Laboratory ID = 20152610011 Lab Value = 0.016 Expected Conc. = 0.0295 Report level label = 0.0048 Pct Recovery = 55% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl SpecificMix = 0406-15-01 Laboratory ID = 20152460215 Lab Value = 0.015 Expected Conc. = 0.0295 Report level label = 0.0048 Pct Recovery = 51% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl SpecificMix = 0406-15-01 Laboratory ID = 20171660002 Lab Value = 0.025 Expected Conc. = 0.024 Report level label = 0.0048 Pct Recovery = 105% Analysis Date = 08/23/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = 060916 Laboratory ID = 20171380001 Lab Value = 0.014 Expected Conc. = 0.024 Report level label = 0.0048 Pct Recovery = 56% Analysis Date = 06/07/17 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 041816 Laboratory ID = 20170740063 Lab Value = 0.018 Expected Conc. = 0.024 Report level label = 0.0048 Pct Recovery = 76% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl SpecificMix = 041816 Laboratory ID = 20170190026 Lab Value = 0.025 Expected Conc. = 0.024 Report level label = 0.0048 Pct Recovery = 103% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = 060916 Laboratory ID = 20161740258 Lab Value = 0.014 Expected Conc. = 0.024 Report level label = 0.0048 Pct Recovery = 56% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 041816 Laboratory ID = 20131370001 Lab Value = 0.020 Expected Conc. = 0.02 Report level label = 0.0048 Pct Recovery = 98% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl SpecificMix = 1473000 Laboratory ID = 20150720069 Lab Value = 0.015 Expected Conc. = 0.0192 Report level label = 0.0048 Pct Recovery = 78% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 03DD006 Laboratory ID = 20143110108 Lab Value = 0.012 Expected Conc. = 0.0192 Report level label = 0.0048 Pct Recovery = 63% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 03DD006 Laboratory ID = 20142960086 Lab Value = 0.014 Expected Conc. = 0.0192 Report level label = 0.0048 Pct Recovery = 74% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 03DD006 Laboratory ID = 20142720002 Lab Value = 0.014 Expected Conc. = 0.0192 Report level label = 0.0048 Pct Recovery = 70% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl SpecificMix = LC06435 Laboratory ID = 20142530087 Lab Value = 0.014 Expected Conc. = 0.0192 Report level label = 0.0048 Pct Recovery = 74% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl SpecificMix = LC06435 Laboratory ID = 20142270001 Lab Value = 0.012 Expected Conc. = 0.0192 Report level label = 0.0048 Pct Recovery = 60% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl SpecificMix = 03DD006 Laboratory ID = 20141570088 Lab Value = 0.018 Expected Conc. = 0.0192 Report level label = 0.0048 Pct Recovery = 94% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl SpecificMix = LC06435 Laboratory ID = 20141220025 Lab Value = 0.017 Expected Conc. = 0.0192 Report level label = 0.0048 Pct Recovery = 91% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl SpecificMix = LC06435 Laboratory ID = 20173480003 Lab Value = 0.016 Expected Conc. = 0.016 Report level label = 0.008 Pct Recovery = 97% Analysis Date = 04/05/18 SpikeMix = Abs 071717Pest: 50 µl & ChemService 6567600: 50 µl SpecificMix = 071717Pest Laboratory ID = 20172370001 Lab Value = 0.013 Expected Conc. = 0.016 Report level label = 0.0048 Pct Recovery = 79% Analysis Date = 11/18/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6537100: 50 µl SpecificMix = 6537100 Laboratory ID = 20172230001 Lab Value = 0.017 Expected Conc. = 0.016 Report level label = 0.0048 Pct Recovery = 105% Analysis Date = 10/19/17 SpikeMix = ChemService 6472100: 50 µl & Abs 071717Pest: 50 µl SpecificMix = 071717Pest Laboratory ID = 20161260151 Lab Value = 0.012 Expected Conc. = 0.016 Report level label = 0.0048 Pct Recovery = 77% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = 3851600 Laboratory ID = 20151550293 Lab Value = 0.009 Expected Conc. = 0.016 Report level label = 0.0048 Pct Recovery = 59% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl SpecificMix = 3851600 Laboratory ID = 20151270112 Lab Value = 0.013 Expected Conc. = 0.016 Report level label = 0.0048 Pct Recovery = 78% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl SpecificMix = 3851600 Laboratory ID = 20160770090 Lab Value = 0.012 Expected Conc. = 0.0148 Report level label = 0.0048 Pct Recovery = 83% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20160630046 Lab Value = 0.011 Expected Conc. = 0.0148 Report level label = 0.0048 Pct Recovery = 76% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20153510109 Lab Value = 0.012 Expected Conc. = 0.0148 Report level label = 0.0048 Pct Recovery = 79% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20153440001 Lab Value = 0.012 Expected Conc. = 0.0148 Report level label = 0.0048 Pct Recovery = 82% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20172020035 Lab Value = 0.014 Expected Conc. = 0.0128 Report level label = 0.0048 Pct Recovery = 110% Analysis Date = 11/07/17 SpikeMix = Abs 071717Pest: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 071717Pest Laboratory ID = 20171940002 Lab Value = 0.009 Expected Conc. = 0.012 Report level label = 0.0048 Pct Recovery = 76% Analysis Date = 11/10/17 SpikeMix = ChemService 5054800: 40 µl & NSI 041816: 40 µl SpecificMix = 041816 Laboratory ID = 20171160110 Lab Value = 0.012 Expected Conc. = 0.012 Report level label = 0.0048 Pct Recovery = 97% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = 060916 Laboratory ID = 20162520001 Lab Value = 0.013 Expected Conc. = 0.012 Report level label = 0.0048 Pct Recovery = 105% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl SpecificMix = 060916 Laboratory ID = 20163560019 Lab Value = 0.011 Expected Conc. = 0.012 Report level label = 0.0048 Pct Recovery = 88% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl SpecificMix = 060916 Laboratory ID = 20162380004 Lab Value = 0.012 Expected Conc. = 0.012 Report level label = 0.0048 Pct Recovery = 101% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = 060916 Laboratory ID = 20162020124 Lab Value = 0.009 Expected Conc. = 0.012 Report level label = 0.0048 Pct Recovery = 77% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl SpecificMix = 041816 Laboratory ID = 20161600087 Lab Value = 0.010 Expected Conc. = 0.012 Report level label = 0.0048 Pct Recovery = 82% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 041816 Laboratory ID = 20161340228 Lab Value = 0.009 Expected Conc. = 0.012 Report level label = 0.0048 Pct Recovery = 72% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl SpecificMix = 041816 Laboratory ID = 20161190075 Lab Value = 0.008 Expected Conc. = 0.012 Report level label = 0.0048 Pct Recovery = 69% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 041816 Laboratory ID = 20180940080 Lab Value = 0.009 Expected Conc. = 0.0096 Report level label = 0.008 Pct Recovery = 94% Analysis Date = 05/31/18 SpikeMix = ChemService 6472100: 30 µl & Abs 071717Pest: 30 µl SpecificMix = 071717Pest Laboratory ID = 20180730064 Lab Value = 0.012 Expected Conc. = 0.0096 Report level label = 0.008 Pct Recovery = 125% Analysis Date = 05/16/18 SpikeMix = Abs 071717Pest: 30 µl & Abs 071817Pest: 30 µl SpecificMix = 071717Pest Laboratory ID = 20173120093 Lab Value = 0.010 Expected Conc. = 0.0096 Report level label = 0.0048 Pct Recovery = 103% Analysis Date = 03/10/18 SpikeMix = ChemService 6472100: 30 µl & ChemService 6537100: 30 µl SpecificMix = 6537100 Laboratory ID = 20172780018 Lab Value = 0.008 Expected Conc. = 0.0096 Report level label = 0.0048 Pct Recovery = 82% Analysis Date = 02/08/18 SpikeMix = ChemService 6537100: 30 µl & Abs 071817Pest: 30 µl SpecificMix = 6537100 Laboratory ID = 20150150115 Lab Value = 0.008 Expected Conc. = 0.0096 Report level label = 0.0048 Pct Recovery = 84% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl SpecificMix = LC06435 Laboratory ID = 20143370094 Lab Value = 0.007 Expected Conc. = 0.0096 Report level label = 0.0048 Pct Recovery = 71% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl SpecificMix = LC06435 Laboratory ID = 20142200164 Lab Value = 0.008 Expected Conc. = 0.0096 Report level label = 0.0048 Pct Recovery = 78% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 03DD006 Laboratory ID = 20141910243 Lab Value = 0.007 Expected Conc. = 0.0096 Report level label = 0.0048 Pct Recovery = 74% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = LC06435 Laboratory ID = 20141840097 Lab Value = 0.008 Expected Conc. = 0.0096 Report level label = 0.0048 Pct Recovery = 86% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl SpecificMix = LC06435 Laboratory ID = 20141640076 Lab Value = 0.007 Expected Conc. = 0.0096 Report level label = 0.0048 Pct Recovery = 76% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = 03DD006 Laboratory ID = 20141420140 Lab Value = 0.008 Expected Conc. = 0.0096 Report level label = 0.0048 Pct Recovery = 86% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 03DD006 Laboratory ID = 20141080004 Lab Value = 0.008 Expected Conc. = 0.0096 Report level label = 0.0048 Pct Recovery = 79% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl SpecificMix = 03DD006 Laboratory ID = 20160430111 Lab Value = 0.008 Expected Conc. = 0.008 Report level label = 0.0048 Pct Recovery = 95% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 3851600 Laboratory ID = 20160210080 Lab Value = 0.007 Expected Conc. = 0.008 Report level label = 0.0048 Pct Recovery = 84% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 3851600 Laboratory ID = 20152950078 Lab Value = 0.006 Expected Conc. = 0.008 Report level label = 0.0048 Pct Recovery = 71% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 3851600 Laboratory ID = 20153030068 Lab Value = 0.008 Expected Conc. = 0.008 Report level label = 0.0048 Pct Recovery = 96% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = 3851600 Laboratory ID = 20151760208 Lab Value = 0.003 Expected Conc. = 0.008 Report level label = 0.0048 Pct Recovery = 32% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl SpecificMix = 3851600 Laboratory ID = 20151380009 Lab Value = 0.005 Expected Conc. = 0.008 Report level label = 0.0048 Pct Recovery = 66% Analysis Date = 05/30/15 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 3851600 Laboratory ID = 20140730138 Lab Value = 0.009 Expected Conc. = 0.008 Report level label = 0.0048 Pct Recovery = 110% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 1473000 Laboratory ID = 20133470008 Lab Value = 0.008 Expected Conc. = 0.008 Report level label = 0.0048 Pct Recovery = 95% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl SpecificMix = 1473000 Laboratory ID = 20133310030 Lab Value = 0.009 Expected Conc. = 0.008 Report level label = 0.0048 Pct Recovery = 114% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl SpecificMix = 1473000 Laboratory ID = 20131790009 Lab Value = 0.008 Expected Conc. = 0.008 Report level label = 0.0048 Pct Recovery = 103% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl SpecificMix = 1473000 Laboratory ID = 20131650073 Lab Value = 0.009 Expected Conc. = 0.008 Report level label = 0.0048 Pct Recovery = 114% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl SpecificMix = 1473000 Laboratory ID = 20152040177 Lab Value = 0.005 Expected Conc. = 0.0074 Report level label = 0.0048 Pct Recovery = 72% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl SpecificMix = 0406-15-01 Analysis Date = 05/31/18 Pct Recovery = 101% Analysis Date = 05/21/18 Pct Recovery = 100% Analysis Date = 05/21/18 Pct Recovery = 100% Analysis Date = 05/11/18 Pct Recovery = 100% Analysis Date = 05/11/18 Pct Recovery = 100% Analysis Date = 05/01/18 Pct Recovery = 100% Analysis Date = 05/01/18 Pct Recovery = 100% Analysis Date = 04/21/18 Pct Recovery = 99% Analysis Date = 04/21/18 Pct Recovery = 99% Analysis Date = 04/11/18 Pct Recovery = 99% Analysis Date = 04/11/18 Pct Recovery = 99% Analysis Date = 04/02/18 Pct Recovery = 99% Analysis Date = 04/02/18 Pct Recovery = 99% Analysis Date = 03/23/18 Pct Recovery = 99% Analysis Date = 03/23/18 Pct Recovery = 99% Analysis Date = 03/13/18 Pct Recovery = 98% Analysis Date = 03/13/18 Pct Recovery = 98% Analysis Date = 03/03/18 Pct Recovery = 98% Analysis Date = 03/03/18 Pct Recovery = 98% Analysis Date = 02/21/18 Pct Recovery = 98% Analysis Date = 02/21/18 Pct Recovery = 98% Analysis Date = 02/12/18 Pct Recovery = 98% Analysis Date = 02/12/18 Pct Recovery = 98% Analysis Date = 02/02/18 Pct Recovery = 97% Analysis Date = 02/02/18 Pct Recovery = 97% Analysis Date = 01/23/18 Pct Recovery = 97% Analysis Date = 01/23/18 Pct Recovery = 97% Analysis Date = 01/13/18 Pct Recovery = 97% Analysis Date = 01/13/18 Pct Recovery = 97% Analysis Date = 01/03/18 Pct Recovery = 96% Analysis Date = 01/03/18 Pct Recovery = 96% Analysis Date = 12/25/17 Pct Recovery = 96% Analysis Date = 12/25/17 Pct Recovery = 96% Analysis Date = 12/15/17 Pct Recovery = 96% Analysis Date = 12/15/17 Pct Recovery = 96% Analysis Date = 12/05/17 Pct Recovery = 96% Analysis Date = 12/05/17 Pct Recovery = 96% Analysis Date = 11/25/17 Pct Recovery = 95% Analysis Date = 11/25/17 Pct Recovery = 95% Analysis Date = 11/15/17 Pct Recovery = 95% Analysis Date = 11/15/17 Pct Recovery = 95% Analysis Date = 11/05/17 Pct Recovery = 95% Analysis Date = 11/05/17 Pct Recovery = 95% Analysis Date = 10/27/17 Pct Recovery = 95% Analysis Date = 10/27/17 Pct Recovery = 95% Analysis Date = 10/17/17 Pct Recovery = 94% Analysis Date = 10/17/17 Pct Recovery = 94% Analysis Date = 10/07/17 Pct Recovery = 94% Analysis Date = 10/07/17 Pct Recovery = 94% Analysis Date = 09/27/17 Pct Recovery = 94% Analysis Date = 09/27/17 Pct Recovery = 94% Analysis Date = 09/17/17 Pct Recovery = 93% Analysis Date = 09/17/17 Pct Recovery = 93% Analysis Date = 09/08/17 Pct Recovery = 93% Analysis Date = 09/08/17 Pct Recovery = 93% Analysis Date = 08/29/17 Pct Recovery = 93% Analysis Date = 08/29/17 Pct Recovery = 93% Analysis Date = 08/19/17 Pct Recovery = 93% Analysis Date = 08/19/17 Pct Recovery = 93% Analysis Date = 08/09/17 Pct Recovery = 92% Analysis Date = 08/09/17 Pct Recovery = 92% Analysis Date = 07/30/17 Pct Recovery = 92% Analysis Date = 07/30/17 Pct Recovery = 92% Analysis Date = 07/21/17 Pct Recovery = 92% Analysis Date = 07/21/17 Pct Recovery = 92% Analysis Date = 07/11/17 Pct Recovery = 91% Analysis Date = 07/11/17 Pct Recovery = 91% Analysis Date = 07/01/17 Pct Recovery = 91% Analysis Date = 07/01/17 Pct Recovery = 91% Analysis Date = 06/21/17 Pct Recovery = 91% Analysis Date = 06/21/17 Pct Recovery = 91% Analysis Date = 06/11/17 Pct Recovery = 91% Analysis Date = 06/11/17 Pct Recovery = 91% Analysis Date = 06/02/17 Pct Recovery = 90% Analysis Date = 06/02/17 Pct Recovery = 90% Analysis Date = 05/23/17 Pct Recovery = 90% Analysis Date = 05/23/17 Pct Recovery = 90% Analysis Date = 05/13/17 Pct Recovery = 90% Analysis Date = 05/13/17 Pct Recovery = 90% Analysis Date = 05/03/17 Pct Recovery = 89% Analysis Date = 05/03/17 Pct Recovery = 89% Analysis Date = 04/23/17 Pct Recovery = 89% Analysis Date = 04/23/17 Pct Recovery = 89% Analysis Date = 04/13/17 Pct Recovery = 89% Analysis Date = 04/13/17 Pct Recovery = 89% Analysis Date = 04/04/17 Pct Recovery = 89% Analysis Date = 04/04/17 Pct Recovery = 89% Analysis Date = 03/25/17 Pct Recovery = 88% Analysis Date = 03/25/17 Pct Recovery = 88% Analysis Date = 03/15/17 Pct Recovery = 88% Analysis Date = 03/15/17 Pct Recovery = 88% Analysis Date = 03/05/17 Pct Recovery = 88% Analysis Date = 03/05/17 Pct Recovery = 88% Analysis Date = 02/23/17 Pct Recovery = 87% Analysis Date = 02/23/17 Pct Recovery = 87% Analysis Date = 02/14/17 Pct Recovery = 87% Analysis Date = 02/14/17 Pct Recovery = 87% Analysis Date = 02/04/17 Pct Recovery = 87% Analysis Date = 02/04/17 Pct Recovery = 87% Analysis Date = 01/25/17 Pct Recovery = 86% Analysis Date = 01/25/17 Pct Recovery = 86% Analysis Date = 01/15/17 Pct Recovery = 86% Analysis Date = 01/15/17 Pct Recovery = 86% Analysis Date = 01/05/17 Pct Recovery = 86% Analysis Date = 01/05/17 Pct Recovery = 86% Analysis Date = 12/27/16 Pct Recovery = 86% Analysis Date = 12/27/16 Pct Recovery = 86% Analysis Date = 12/17/16 Pct Recovery = 85% Analysis Date = 12/17/16 Pct Recovery = 85% Analysis Date = 12/07/16 Pct Recovery = 85% Analysis Date = 12/07/16 Pct Recovery = 85% Analysis Date = 11/27/16 Pct Recovery = 85% Analysis Date = 11/27/16 Pct Recovery = 85% Analysis Date = 11/17/16 Pct Recovery = 84% Analysis Date = 11/17/16 Pct Recovery = 84% Analysis Date = 11/08/16 Pct Recovery = 84% Analysis Date = 11/08/16 Pct Recovery = 84% Analysis Date = 10/29/16 Pct Recovery = 84% Analysis Date = 10/29/16 Pct Recovery = 84% Analysis Date = 10/19/16 Pct Recovery = 83% Analysis Date = 10/19/16 Pct Recovery = 83% Analysis Date = 10/09/16 Pct Recovery = 83% Analysis Date = 10/09/16 Pct Recovery = 83% Analysis Date = 09/29/16 Pct Recovery = 83% Analysis Date = 09/29/16 Pct Recovery = 83% Analysis Date = 09/19/16 Pct Recovery = 83% Analysis Date = 09/19/16 Pct Recovery = 83% Analysis Date = 09/10/16 Pct Recovery = 82% Analysis Date = 09/10/16 Pct Recovery = 82% Analysis Date = 08/31/16 Pct Recovery = 82% Analysis Date = 08/31/16 Pct Recovery = 82% Analysis Date = 08/21/16 Pct Recovery = 82% Analysis Date = 08/21/16 Pct Recovery = 82% Analysis Date = 08/11/16 Pct Recovery = 81% Analysis Date = 08/11/16 Pct Recovery = 81% Analysis Date = 08/01/16 Pct Recovery = 81% Analysis Date = 08/01/16 Pct Recovery = 81% Analysis Date = 07/23/16 Pct Recovery = 81% Analysis Date = 07/23/16 Pct Recovery = 81% Analysis Date = 07/13/16 Pct Recovery = 80% Analysis Date = 07/13/16 Pct Recovery = 80% Analysis Date = 07/03/16 Pct Recovery = 80% Analysis Date = 07/03/16 Pct Recovery = 80% Analysis Date = 06/23/16 Pct Recovery = 80% Analysis Date = 06/23/16 Pct Recovery = 80% Analysis Date = 06/13/16 Pct Recovery = 79% Analysis Date = 06/13/16 Pct Recovery = 79% Analysis Date = 06/04/16 Pct Recovery = 79% Analysis Date = 06/04/16 Pct Recovery = 79% Analysis Date = 05/25/16 Pct Recovery = 79% Analysis Date = 05/25/16 Pct Recovery = 79% Analysis Date = 05/15/16 Pct Recovery = 79% Analysis Date = 05/15/16 Pct Recovery = 79% Analysis Date = 05/05/16 Pct Recovery = 78% Analysis Date = 05/05/16 Pct Recovery = 78% Analysis Date = 04/25/16 Pct Recovery = 78% Analysis Date = 04/25/16 Pct Recovery = 78% Analysis Date = 04/16/16 Pct Recovery = 78% Analysis Date = 04/16/16 Pct Recovery = 78% Analysis Date = 04/06/16 Pct Recovery = 77% Analysis Date = 04/06/16 Pct Recovery = 77% Analysis Date = 03/27/16 Pct Recovery = 77% Analysis Date = 03/27/16 Pct Recovery = 77% Analysis Date = 03/17/16 Pct Recovery = 77% Analysis Date = 03/17/16 Pct Recovery = 77% Analysis Date = 03/07/16 Pct Recovery = 76% Analysis Date = 03/07/16 Pct Recovery = 76% Analysis Date = 02/26/16 Pct Recovery = 76% Analysis Date = 02/26/16 Pct Recovery = 76% Analysis Date = 02/17/16 Pct Recovery = 76% Analysis Date = 02/17/16 Pct Recovery = 76% Analysis Date = 02/07/16 Pct Recovery = 75% Analysis Date = 02/07/16 Pct Recovery = 75% Analysis Date = 01/28/16 Pct Recovery = 75% Analysis Date = 01/28/16 Pct Recovery = 75% Analysis Date = 01/18/16 Pct Recovery = 75% Analysis Date = 01/18/16 Pct Recovery = 75% Analysis Date = 01/08/16 Pct Recovery = 75% Analysis Date = 01/08/16 Pct Recovery = 75% Analysis Date = 12/30/15 Pct Recovery = 75% Analysis Date = 12/30/15 Pct Recovery = 75% Analysis Date = 12/20/15 Pct Recovery = 74% Analysis Date = 12/20/15 Pct Recovery = 74% Analysis Date = 12/10/15 Pct Recovery = 74% Analysis Date = 12/10/15 Pct Recovery = 74% Analysis Date = 11/30/15 Pct Recovery = 74% Analysis Date = 11/30/15 Pct Recovery = 74% Analysis Date = 11/20/15 Pct Recovery = 74% Analysis Date = 11/20/15 Pct Recovery = 74% Analysis Date = 11/11/15 Pct Recovery = 74% Analysis Date = 11/11/15 Pct Recovery = 74% Analysis Date = 11/01/15 Pct Recovery = 74% Analysis Date = 11/01/15 Pct Recovery = 74% Analysis Date = 10/22/15 Pct Recovery = 74% Analysis Date = 10/22/15 Pct Recovery = 74% Analysis Date = 10/12/15 Pct Recovery = 74% Analysis Date = 10/12/15 Pct Recovery = 74% Analysis Date = 10/02/15 Pct Recovery = 74% Analysis Date = 10/02/15 Pct Recovery = 74% Analysis Date = 09/23/15 Pct Recovery = 74% Analysis Date = 09/23/15 Pct Recovery = 74% Analysis Date = 09/13/15 Pct Recovery = 74% Analysis Date = 09/13/15 Pct Recovery = 74% Analysis Date = 09/03/15 Pct Recovery = 73% Analysis Date = 09/03/15 Pct Recovery = 73% Analysis Date = 08/24/15 Pct Recovery = 73% Analysis Date = 08/24/15 Pct Recovery = 73% Analysis Date = 08/14/15 Pct Recovery = 73% Analysis Date = 08/14/15 Pct Recovery = 73% Analysis Date = 08/04/15 Pct Recovery = 73% Analysis Date = 08/04/15 Pct Recovery = 73% Analysis Date = 07/26/15 Pct Recovery = 73% Analysis Date = 07/26/15 Pct Recovery = 73% Analysis Date = 07/16/15 Pct Recovery = 73% Analysis Date = 07/16/15 Pct Recovery = 73% Analysis Date = 07/06/15 Pct Recovery = 73% Analysis Date = 07/06/15 Pct Recovery = 73% Analysis Date = 06/26/15 Pct Recovery = 73% Analysis Date = 06/26/15 Pct Recovery = 73% Analysis Date = 06/16/15 Pct Recovery = 73% Analysis Date = 06/16/15 Pct Recovery = 73% Analysis Date = 06/07/15 Pct Recovery = 73% Analysis Date = 06/07/15 Pct Recovery = 73% Analysis Date = 05/28/15 Pct Recovery = 74% Analysis Date = 05/28/15 Pct Recovery = 74% Analysis Date = 05/18/15 Pct Recovery = 74% Analysis Date = 05/18/15 Pct Recovery = 74% Analysis Date = 05/08/15 Pct Recovery = 74% Analysis Date = 05/08/15 Pct Recovery = 74% Analysis Date = 04/28/15 Pct Recovery = 74% Analysis Date = 04/28/15 Pct Recovery = 74% Analysis Date = 04/19/15 Pct Recovery = 74% Analysis Date = 04/19/15 Pct Recovery = 74% Analysis Date = 04/09/15 Pct Recovery = 74% Analysis Date = 04/09/15 Pct Recovery = 74% Analysis Date = 03/30/15 Pct Recovery = 74% Analysis Date = 03/30/15 Pct Recovery = 74% Analysis Date = 03/20/15 Pct Recovery = 74% Analysis Date = 03/20/15 Pct Recovery = 74% Analysis Date = 03/10/15 Pct Recovery = 75% Analysis Date = 03/10/15 Pct Recovery = 75% Analysis Date = 02/28/15 Pct Recovery = 75% Analysis Date = 02/28/15 Pct Recovery = 75% Analysis Date = 02/19/15 Pct Recovery = 75% Analysis Date = 02/19/15 Pct Recovery = 75% Analysis Date = 02/09/15 Pct Recovery = 75% Analysis Date = 02/09/15 Pct Recovery = 75% Analysis Date = 01/30/15 Pct Recovery = 75% Analysis Date = 01/30/15 Pct Recovery = 75% Analysis Date = 01/20/15 Pct Recovery = 75% Analysis Date = 01/20/15 Pct Recovery = 75% Analysis Date = 01/10/15 Pct Recovery = 75% Analysis Date = 01/10/15 Pct Recovery = 75% Analysis Date = 01/01/15 Pct Recovery = 76% Analysis Date = 01/01/15 Pct Recovery = 76% Analysis Date = 12/22/14 Pct Recovery = 76% Analysis Date = 12/22/14 Pct Recovery = 76% Analysis Date = 12/12/14 Pct Recovery = 76% Analysis Date = 12/12/14 Pct Recovery = 76% Analysis Date = 12/02/14 Pct Recovery = 76% Analysis Date = 12/02/14 Pct Recovery = 76% Analysis Date = 11/22/14 Pct Recovery = 76% Analysis Date = 11/22/14 Pct Recovery = 76% Analysis Date = 11/13/14 Pct Recovery = 76% Analysis Date = 11/13/14 Pct Recovery = 76% Analysis Date = 11/03/14 Pct Recovery = 76% Analysis Date = 11/03/14 Pct Recovery = 76% Analysis Date = 10/24/14 Pct Recovery = 76% Analysis Date = 10/24/14 Pct Recovery = 76% Analysis Date = 10/14/14 Pct Recovery = 77% Analysis Date = 10/14/14 Pct Recovery = 77% Analysis Date = 10/04/14 Pct Recovery = 77% Analysis Date = 10/04/14 Pct Recovery = 77% Analysis Date = 09/25/14 Pct Recovery = 77% Analysis Date = 09/25/14 Pct Recovery = 77% Analysis Date = 09/15/14 Pct Recovery = 78% Analysis Date = 09/15/14 Pct Recovery = 78% Analysis Date = 09/05/14 Pct Recovery = 78% Analysis Date = 09/05/14 Pct Recovery = 78% Analysis Date = 08/26/14 Pct Recovery = 79% Analysis Date = 08/26/14 Pct Recovery = 79% Analysis Date = 08/16/14 Pct Recovery = 79% Analysis Date = 08/16/14 Pct Recovery = 79% Analysis Date = 08/06/14 Pct Recovery = 80% Analysis Date = 08/06/14 Pct Recovery = 80% Analysis Date = 07/28/14 Pct Recovery = 80% Analysis Date = 07/28/14 Pct Recovery = 80% Analysis Date = 07/18/14 Pct Recovery = 81% Analysis Date = 07/18/14 Pct Recovery = 81% Analysis Date = 07/08/14 Pct Recovery = 81% Analysis Date = 07/08/14 Pct Recovery = 81% Analysis Date = 06/28/14 Pct Recovery = 81% Analysis Date = 06/28/14 Pct Recovery = 81% Analysis Date = 06/18/14 Pct Recovery = 82% Analysis Date = 06/18/14 Pct Recovery = 82% Analysis Date = 06/09/14 Pct Recovery = 82% Analysis Date = 06/09/14 Pct Recovery = 82% Analysis Date = 05/30/14 Pct Recovery = 82% Analysis Date = 05/30/14 Pct Recovery = 82% Analysis Date = 05/20/14 Pct Recovery = 83% Analysis Date = 05/20/14 Pct Recovery = 83% Analysis Date = 05/10/14 Pct Recovery = 83% Analysis Date = 05/10/14 Pct Recovery = 83% Analysis Date = 04/30/14 Pct Recovery = 84% Analysis Date = 04/30/14 Pct Recovery = 84% Analysis Date = 04/21/14 Pct Recovery = 84% Analysis Date = 04/21/14 Pct Recovery = 84% Analysis Date = 04/11/14 Pct Recovery = 84% Analysis Date = 04/11/14 Pct Recovery = 84% Analysis Date = 04/01/14 Pct Recovery = 85% Analysis Date = 04/01/14 Pct Recovery = 85% Analysis Date = 03/22/14 Pct Recovery = 85% Analysis Date = 03/22/14 Pct Recovery = 85% Analysis Date = 03/12/14 Pct Recovery = 86% Analysis Date = 03/12/14 Pct Recovery = 86% Analysis Date = 03/03/14 Pct Recovery = 86% Analysis Date = 03/03/14 Pct Recovery = 86% Analysis Date = 02/21/14 Pct Recovery = 86% Analysis Date = 02/21/14 Pct Recovery = 86% Analysis Date = 02/11/14 Pct Recovery = 87% Analysis Date = 02/11/14 Pct Recovery = 87% Analysis Date = 02/01/14 Pct Recovery = 87% Analysis Date = 02/01/14 Pct Recovery = 87% Analysis Date = 01/22/14 Pct Recovery = 88% Analysis Date = 01/22/14 Pct Recovery = 88% Analysis Date = 01/12/14 Pct Recovery = 88% Analysis Date = 01/12/14 Pct Recovery = 88% Analysis Date = 01/03/14 Pct Recovery = 88% Analysis Date = 01/03/14 Pct Recovery = 88% Analysis Date = 12/24/13 Pct Recovery = 89% Analysis Date = 12/24/13 Pct Recovery = 89% Analysis Date = 12/14/13 Pct Recovery = 89% Analysis Date = 12/14/13 Pct Recovery = 89% Analysis Date = 12/04/13 Pct Recovery = 89% Analysis Date = 12/04/13 Pct Recovery = 89% Analysis Date = 11/24/13 Pct Recovery = 90% Analysis Date = 11/24/13 Pct Recovery = 90% Analysis Date = 11/15/13 Pct Recovery = 90% Analysis Date = 11/15/13 Pct Recovery = 90% Analysis Date = 11/05/13 Pct Recovery = 91% Analysis Date = 11/05/13 Pct Recovery = 91% Analysis Date = 10/26/13 Pct Recovery = 91% Analysis Date = 10/26/13 Pct Recovery = 91% Analysis Date = 10/16/13 Pct Recovery = 91% Analysis Date = 10/16/13 Pct Recovery = 91% Analysis Date = 10/06/13 Pct Recovery = 92% Analysis Date = 10/06/13 Pct Recovery = 92% Analysis Date = 09/27/13 Pct Recovery = 92% Analysis Date = 09/27/13 Pct Recovery = 92% Analysis Date = 09/17/13 Pct Recovery = 93% Analysis Date = 09/17/13 Pct Recovery = 93% Analysis Date = 09/07/13 Pct Recovery = 93% Analysis Date = 09/07/13 Pct Recovery = 93% Analysis Date = 08/28/13 Pct Recovery = 93% Analysis Date = 08/28/13 Pct Recovery = 93% Analysis Date = 08/18/13 Pct Recovery = 94% Analysis Date = 08/18/13 Pct Recovery = 94% Analysis Date = 08/09/13 Pct Recovery = 94% Analysis Date = 08/09/13 Pct Recovery = 94% Analysis Date = 07/30/13 Pct Recovery = 94% Analysis Date = 07/30/13 Pct Recovery = 94% Analysis Date = 07/20/13 Pct Recovery = 95% Analysis Date = 07/20/13 Pct Recovery = 95% Analysis Date = 07/10/13 Pct Recovery = 95% Analysis Date = 07/10/13 Pct Recovery = 95% Analysis Date = 06/30/13 Pct Recovery = 96% Analysis Date = 06/30/13 Pct Recovery = 96% Analysis Date = 06/20/13 Pct Recovery = 96% Analysis Date = 06/20/13 Pct Recovery = 96% Analysis Date = 06/11/13 Pct Recovery = 96% Analysis Date = 06/11/13 Pct Recovery = 96% Analysis Date = 06/01/13 Pct Recovery = 97% Analysis Date = 06/01/13 Pct Recovery = 97% Analysis Date = 05/22/13 Pct Recovery = 97% Analysis Date = 05/22/13 Pct Recovery = 97% Analysis Date = 05/12/13 Pct Recovery = 97% Analysis Date = 05/12/13 Pct Recovery = 97% Analysis Date = 05/02/13 Pct Recovery = 98% Analysis Date = 05/02/13 Pct Recovery = 98% Analysis Date = 04/23/13 Pct Recovery = 98% Analysis Date = 04/23/13 Pct Recovery = 98% Analysis Date = 04/13/13 Pct Recovery = 99% Analysis Date = 04/13/13 Pct Recovery = 99% Analysis Date = 04/03/13 Pct Recovery = 99% Analysis Date = 04/03/13 Pct Recovery = 99% Analysis Date = 03/24/13 Pct Recovery = 99% Analysis Date = 03/24/13 Pct Recovery = 99% Analysis Date = 03/14/13 Pct Recovery = 100% Analysis Date = 03/14/13 Pct Recovery = 100% Analysis Date = 03/05/13 Pct Recovery = 100% Analysis Date = 03/05/13 Pct Recovery = 100% Analysis Date = 02/23/13 Pct Recovery = 100% Analysis Date = 02/23/13 Pct Recovery = 100% Analysis Date = 02/13/13 Pct Recovery = 101% Analysis Date = 02/13/13 Pct Recovery = 101% Analysis Date = 02/03/13 Pct Recovery = 101% Analysis Date = 02/03/13 Pct Recovery = 101% Analysis Date = 01/24/13 Pct Recovery = 102% Analysis Date = 01/24/13 Pct Recovery = 102% Analysis Date = 01/15/13 Pct Recovery = 102% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
FONOFOS

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 76 85% 17% 84% 16%
Total 76 85% 17% 84% 16%

Sample Statistics
FONOFOS

Characteristic N % % Basis
Plotted 76 99% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 77 .  
False Negatives 1 1% 1 out of 77
Not Spiked 51 .  
False Positives 0 0% 0 out of 51

OBSP Determination:
HEXAZINONE
METHOD: 2033 , TESTIDCODE: 04025GCM39

Laboratory ID = 20130940097 Lab Value = 0.109 Expected Conc. = 0.3 Report level label = 0.012 Pct Recovery = 36% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = 0507-12-04.2 Laboratory ID = 20130810108 Lab Value = 0.134 Expected Conc. = 0.3 Report level label = 0.012 Pct Recovery = 45% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl SpecificMix = LB92783 Laboratory ID = 20130100066 Lab Value = 0.142 Expected Conc. = 0.3 Report level label = 0.012 Pct Recovery = 47% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl SpecificMix = LB92783 Laboratory ID = 20123560092 Lab Value = 0.118 Expected Conc. = 0.3 Report level label = 0.012 Pct Recovery = 39% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = 0507-12-04.2 Laboratory ID = 20132490342 Lab Value = 0.084 Expected Conc. = 0.2 Report level label = 0.012 Pct Recovery = 42% Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20130510051 Lab Value = 0.062 Expected Conc. = 0.12 Report level label = 0.012 Pct Recovery = 51% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl SpecificMix = 0507-12-04.2 Laboratory ID = 20130390105 Lab Value = 0.049 Expected Conc. = 0.12 Report level label = 0.012 Pct Recovery = 41% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl SpecificMix = LB92783 Laboratory ID = 20132140002 Lab Value = 0.046 Expected Conc. = 0.1004 Report level label = 0.012 Pct Recovery = 46% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl SpecificMix = LB99392 Laboratory ID = 20131370001 Lab Value = 0.079 Expected Conc. = 0.1004 Report level label = 0.012 Pct Recovery = 78% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl SpecificMix = LB99392 Laboratory ID = 20140370077 Lab Value = 0.035 Expected Conc. = 0.1 Report level label = 0.012 Pct Recovery = 35% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20132560001 Lab Value = 0.051 Expected Conc. = 0.1 Report level label = 0.012 Pct Recovery = 51% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20172510330 Lab Value = 0.044 Expected Conc. = 0.081 Report level label = 0.012 Pct Recovery = 54% Analysis Date = 12/29/17 SpikeMix = ChemService 6537100: 100 µl & Abs 071817Pest: 100 µl SpecificMix = 6537100 Laboratory ID = 20180390003 Lab Value = 0.052 Expected Conc. = 0.08 Report level label = 0.012 Pct Recovery = 65% Analysis Date = 04/06/18 SpikeMix = Spex Organics EN170808006: 100 µl & Abs 071717Pest: 100 µl SpecificMix = 071717Pest Laboratory ID = 20161880109 Lab Value = 0.058 Expected Conc. = 0.075 Report level label = 0.012 Pct Recovery = 77% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl SpecificMix = 03FF076 Laboratory ID = 20163370001 Lab Value = 0.048 Expected Conc. = 0.0746 Report level label = 0.012 Pct Recovery = 65% Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl SpecificMix = B20160331 Laboratory ID = 20163150006 Lab Value = 0.047 Expected Conc. = 0.0746 Report level label = 0.012 Pct Recovery = 63% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl SpecificMix = B20160331 Laboratory ID = 20152610011 Lab Value = 0.021 Expected Conc. = 0.0725 Report level label = 0.012 Pct Recovery = 29% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl SpecificMix = 0406-15-01 Laboratory ID = 20152460215 Lab Value = 0.047 Expected Conc. = 0.0725 Report level label = 0.012 Pct Recovery = 65% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl SpecificMix = 0406-15-01 Laboratory ID = 20172020035 Lab Value = 0.049 Expected Conc. = 0.062 Report level label = 0.012 Pct Recovery = 78% Analysis Date = 11/07/17 SpikeMix = Abs 071717Pest: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20170960001 Lab Value = 0.036 Expected Conc. = 0.06 Report level label = 0.012 Pct Recovery = 60% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl SpecificMix = 03FF076 Laboratory ID = 20171720140 Lab Value = 0.038 Expected Conc. = 0.0597 Report level label = 0.012 Pct Recovery = 64% Analysis Date = 08/31/17 SpikeMix = Supelco LC20138V: 80 µl & Phenova B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20171660002 Lab Value = 0.041 Expected Conc. = 0.0597 Report level label = 0.012 Pct Recovery = 69% Analysis Date = 08/23/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20170190026 Lab Value = 0.035 Expected Conc. = 0.0597 Report level label = 0.012 Pct Recovery = 59% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20161470001 Lab Value = 0.038 Expected Conc. = 0.0597 Report level label = 0.012 Pct Recovery = 64% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20150430092 Lab Value = 0.009 Expected Conc. = 0.048 Report level label = 0.012 Pct Recovery = 19% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl SpecificMix = E1140407002 Laboratory ID = 20143240095 Lab Value = 0.027 Expected Conc. = 0.048 Report level label = 0.012 Pct Recovery = 56% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl SpecificMix = 032714 Laboratory ID = 20143110108 Lab Value = 0.017 Expected Conc. = 0.048 Report level label = 0.012 Pct Recovery = 34% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl SpecificMix = E1140407002 Laboratory ID = 20142720002 Lab Value = 0.027 Expected Conc. = 0.048 Report level label = 0.012 Pct Recovery = 57% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl SpecificMix = E1140407002 Laboratory ID = 20142270001 Lab Value = 0.022 Expected Conc. = 0.048 Report level label = 0.012 Pct Recovery = 46% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl SpecificMix = 032714 Laboratory ID = 20141770149 Lab Value = 0.027 Expected Conc. = 0.048 Report level label = 0.012 Pct Recovery = 56% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl SpecificMix = E1140407002 Laboratory ID = 20141220025 Lab Value = 0.021 Expected Conc. = 0.048 Report level label = 0.012 Pct Recovery = 45% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl SpecificMix = 032714 Laboratory ID = 20172370001 Lab Value = 0.030 Expected Conc. = 0.0405 Report level label = 0.012 Pct Recovery = 73% Analysis Date = 11/18/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6537100: 50 µl SpecificMix = 6537100 Laboratory ID = 20140510043 Lab Value = 0.032 Expected Conc. = 0.0402 Report level label = 0.012 Pct Recovery = 80% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl SpecificMix = LB99392 Laboratory ID = 20133470008 Lab Value = 0.017 Expected Conc. = 0.0402 Report level label = 0.012 Pct Recovery = 43% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl SpecificMix = LB99392 Laboratory ID = 20133190012 Lab Value = 0.028 Expected Conc. = 0.0402 Report level label = 0.012 Pct Recovery = 70% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = LB99392 Laboratory ID = 20133050050 Lab Value = 0.031 Expected Conc. = 0.0402 Report level label = 0.012 Pct Recovery = 77% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl SpecificMix = LB99392 Laboratory ID = 20173480003 Lab Value = 0.030 Expected Conc. = 0.04 Report level label = 0.012 Pct Recovery = 74% Analysis Date = 04/05/18 SpikeMix = Abs 071717Pest: 50 µl & ChemService 6567600: 50 µl SpecificMix = 071717Pest Laboratory ID = 20172230001 Lab Value = 0.031 Expected Conc. = 0.04 Report level label = 0.012 Pct Recovery = 78% Analysis Date = 10/19/17 SpikeMix = ChemService 6472100: 50 µl & Abs 071717Pest: 50 µl SpecificMix = 071717Pest Laboratory ID = 20133580036 Lab Value = 0.012 Expected Conc. = 0.04 Report level label = 0.012 Pct Recovery = 31% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20131790009 Lab Value = 0.013 Expected Conc. = 0.04 Report level label = 0.012 Pct Recovery = 32% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20131510026 Lab Value = 0.030 Expected Conc. = 0.04 Report level label = 0.012 Pct Recovery = 76% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20160770090 Lab Value = 0.020 Expected Conc. = 0.0362 Report level label = 0.012 Pct Recovery = 56% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20160630046 Lab Value = 0.022 Expected Conc. = 0.0362 Report level label = 0.012 Pct Recovery = 62% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20153510109 Lab Value = 0.021 Expected Conc. = 0.0362 Report level label = 0.012 Pct Recovery = 57% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20153440001 Lab Value = 0.017 Expected Conc. = 0.0362 Report level label = 0.012 Pct Recovery = 48% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20161260151 Lab Value = 0.022 Expected Conc. = 0.036 Report level label = 0.012 Pct Recovery = 60% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = 3851600 Laboratory ID = 20151550293 Lab Value = 0.032 Expected Conc. = 0.036 Report level label = 0.012 Pct Recovery = 89% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl SpecificMix = 3851600 Laboratory ID = 20151270112 Lab Value = 0.025 Expected Conc. = 0.036 Report level label = 0.012 Pct Recovery = 68% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl SpecificMix = 3851600 Laboratory ID = 20171510080 Lab Value = 0.026 Expected Conc. = 0.03 Report level label = 0.012 Pct Recovery = 86% Analysis Date = 06/09/17 SpikeMix = Supelco LC20138V: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20170460061 Lab Value = 0.018 Expected Conc. = 0.03 Report level label = 0.012 Pct Recovery = 60% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl SpecificMix = 03FF076 Laboratory ID = 20162660005 Lab Value = 0.026 Expected Conc. = 0.03 Report level label = 0.012 Pct Recovery = 85% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl SpecificMix = 03FF076 Laboratory ID = 20161600087 Lab Value = 0.020 Expected Conc. = 0.03 Report level label = 0.012 Pct Recovery = 66% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20161340228 Lab Value = 0.021 Expected Conc. = 0.03 Report level label = 0.012 Pct Recovery = 69% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl SpecificMix = 03FF076 Laboratory ID = 20161190075 Lab Value = 0.018 Expected Conc. = 0.03 Report level label = 0.012 Pct Recovery = 61% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20171160110 Lab Value = 0.026 Expected Conc. = 0.0298 Report level label = 0.012 Pct Recovery = 87% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = B20160331 Laboratory ID = 20162380004 Lab Value = 0.019 Expected Conc. = 0.0298 Report level label = 0.012 Pct Recovery = 63% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = B20160331 Laboratory ID = 20162150213 Lab Value = 0.022 Expected Conc. = 0.0298 Report level label = 0.012 Pct Recovery = 75% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl SpecificMix = B20160331 Laboratory ID = 20173120093 Lab Value = 0.019 Expected Conc. = 0.0243 Report level label = 0.012 Pct Recovery = 78% Analysis Date = 03/10/18 SpikeMix = ChemService 6472100: 30 µl & ChemService 6537100: 30 µl SpecificMix = 6537100 Laboratory ID = 20172780018 Lab Value = 0.020 Expected Conc. = 0.0243 Report level label = 0.012 Pct Recovery = 81% Analysis Date = 02/08/18 SpikeMix = ChemService 6537100: 30 µl & Abs 071817Pest: 30 µl SpecificMix = 6537100 Laboratory ID = 20180940080 Lab Value = 0.016 Expected Conc. = 0.024 Report level label = 0.012 Pct Recovery = 67% Analysis Date = 05/31/18 SpikeMix = ChemService 6472100: 30 µl & Abs 071717Pest: 30 µl SpecificMix = 071717Pest Laboratory ID = 20180730064 Lab Value = 0.024 Expected Conc. = 0.024 Report level label = 0.012 Pct Recovery = 100% Analysis Date = 05/16/18 SpikeMix = Abs 071717Pest: 30 µl & Abs 071817Pest: 30 µl SpecificMix = 071717Pest Laboratory ID = 20150150115 Lab Value = 0.022 Expected Conc. = 0.024 Report level label = 0.012 Pct Recovery = 90% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl SpecificMix = 032714 Laboratory ID = 20142820151 Lab Value = 0.017 Expected Conc. = 0.024 Report level label = 0.012 Pct Recovery = 70% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl SpecificMix = 032714 Laboratory ID = 20142470041 Lab Value = 0.012 Expected Conc. = 0.024 Report level label = 0.012 Pct Recovery = 50% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141910243 Lab Value = 0.011 Expected Conc. = 0.024 Report level label = 0.012 Pct Recovery = 45% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141640076 Lab Value = 0.010 Expected Conc. = 0.024 Report level label = 0.012 Pct Recovery = 40% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141490205 Lab Value = 0.014 Expected Conc. = 0.024 Report level label = 0.012 Pct Recovery = 57% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = 032714 Laboratory ID = 20141360094 Lab Value = 0.011 Expected Conc. = 0.024 Report level label = 0.012 Pct Recovery = 47% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141080004 Lab Value = 0.013 Expected Conc. = 0.024 Report level label = 0.012 Pct Recovery = 54% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl SpecificMix = 032714 Laboratory ID = 20152190003 Lab Value = 0.018 Expected Conc. = 0.0181 Report level label = 0.012 Pct Recovery = 98% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = 0406-15-01 Laboratory ID = 20152040177 Lab Value = 0.016 Expected Conc. = 0.0181 Report level label = 0.012 Pct Recovery = 90% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl SpecificMix = 0406-15-01 Laboratory ID = 20160430111 Lab Value = 0.012 Expected Conc. = 0.018 Report level label = 0.012 Pct Recovery = 68% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 3851600 Laboratory ID = 20160210080 Lab Value = 0.012 Expected Conc. = 0.018 Report level label = 0.012 Pct Recovery = 68% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 3851600 Laboratory ID = 20152950078 Lab Value = 0.009 Expected Conc. = 0.018 Report level label = 0.012 Pct Recovery = 52% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 3851600 Laboratory ID = 20153030068 Lab Value = 0.011 Expected Conc. = 0.018 Report level label = 0.012 Pct Recovery = 63% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = 3851600 Laboratory ID = 20151760208 Lab Value = 0.026 Expected Conc. = 0.018 Report level label = 0.012 Pct Recovery = 147% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl SpecificMix = 3851600 Laboratory ID = 20151380009 Lab Value = 0.013 Expected Conc. = 0.018 Report level label = 0.012 Pct Recovery = 73% Analysis Date = 05/30/15 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 3851600 Analysis Date = 05/31/18 Pct Recovery = 76% Analysis Date = 05/21/18 Pct Recovery = 76% Analysis Date = 05/21/18 Pct Recovery = 76% Analysis Date = 05/11/18 Pct Recovery = 76% Analysis Date = 05/11/18 Pct Recovery = 76% Analysis Date = 05/01/18 Pct Recovery = 76% Analysis Date = 05/01/18 Pct Recovery = 76% Analysis Date = 04/21/18 Pct Recovery = 75% Analysis Date = 04/21/18 Pct Recovery = 75% Analysis Date = 04/11/18 Pct Recovery = 75% Analysis Date = 04/11/18 Pct Recovery = 75% Analysis Date = 04/02/18 Pct Recovery = 75% Analysis Date = 04/02/18 Pct Recovery = 75% Analysis Date = 03/23/18 Pct Recovery = 75% Analysis Date = 03/23/18 Pct Recovery = 75% Analysis Date = 03/13/18 Pct Recovery = 75% Analysis Date = 03/13/18 Pct Recovery = 75% Analysis Date = 03/03/18 Pct Recovery = 75% Analysis Date = 03/03/18 Pct Recovery = 75% Analysis Date = 02/21/18 Pct Recovery = 75% Analysis Date = 02/21/18 Pct Recovery = 75% Analysis Date = 02/12/18 Pct Recovery = 74% Analysis Date = 02/12/18 Pct Recovery = 74% Analysis Date = 02/02/18 Pct Recovery = 74% Analysis Date = 02/02/18 Pct Recovery = 74% Analysis Date = 01/23/18 Pct Recovery = 74% Analysis Date = 01/23/18 Pct Recovery = 74% Analysis Date = 01/13/18 Pct Recovery = 74% Analysis Date = 01/13/18 Pct Recovery = 74% Analysis Date = 01/03/18 Pct Recovery = 74% Analysis Date = 01/03/18 Pct Recovery = 74% Analysis Date = 12/25/17 Pct Recovery = 74% Analysis Date = 12/25/17 Pct Recovery = 74% Analysis Date = 12/15/17 Pct Recovery = 73% Analysis Date = 12/15/17 Pct Recovery = 73% Analysis Date = 12/05/17 Pct Recovery = 73% Analysis Date = 12/05/17 Pct Recovery = 73% Analysis Date = 11/25/17 Pct Recovery = 73% Analysis Date = 11/25/17 Pct Recovery = 73% Analysis Date = 11/15/17 Pct Recovery = 73% Analysis Date = 11/15/17 Pct Recovery = 73% Analysis Date = 11/05/17 Pct Recovery = 73% Analysis Date = 11/05/17 Pct Recovery = 73% Analysis Date = 10/27/17 Pct Recovery = 73% Analysis Date = 10/27/17 Pct Recovery = 73% Analysis Date = 10/17/17 Pct Recovery = 73% Analysis Date = 10/17/17 Pct Recovery = 73% Analysis Date = 10/07/17 Pct Recovery = 72% Analysis Date = 10/07/17 Pct Recovery = 72% Analysis Date = 09/27/17 Pct Recovery = 72% Analysis Date = 09/27/17 Pct Recovery = 72% Analysis Date = 09/17/17 Pct Recovery = 72% Analysis Date = 09/17/17 Pct Recovery = 72% Analysis Date = 09/08/17 Pct Recovery = 72% Analysis Date = 09/08/17 Pct Recovery = 72% Analysis Date = 08/29/17 Pct Recovery = 72% Analysis Date = 08/29/17 Pct Recovery = 72% Analysis Date = 08/19/17 Pct Recovery = 72% Analysis Date = 08/19/17 Pct Recovery = 72% Analysis Date = 08/09/17 Pct Recovery = 72% Analysis Date = 08/09/17 Pct Recovery = 72% Analysis Date = 07/30/17 Pct Recovery = 71% Analysis Date = 07/30/17 Pct Recovery = 71% Analysis Date = 07/21/17 Pct Recovery = 71% Analysis Date = 07/21/17 Pct Recovery = 71% Analysis Date = 07/11/17 Pct Recovery = 71% Analysis Date = 07/11/17 Pct Recovery = 71% Analysis Date = 07/01/17 Pct Recovery = 71% Analysis Date = 07/01/17 Pct Recovery = 71% Analysis Date = 06/21/17 Pct Recovery = 71% Analysis Date = 06/21/17 Pct Recovery = 71% Analysis Date = 06/11/17 Pct Recovery = 71% Analysis Date = 06/11/17 Pct Recovery = 71% Analysis Date = 06/02/17 Pct Recovery = 70% Analysis Date = 06/02/17 Pct Recovery = 70% Analysis Date = 05/23/17 Pct Recovery = 70% Analysis Date = 05/23/17 Pct Recovery = 70% Analysis Date = 05/13/17 Pct Recovery = 70% Analysis Date = 05/13/17 Pct Recovery = 70% Analysis Date = 05/03/17 Pct Recovery = 70% Analysis Date = 05/03/17 Pct Recovery = 70% Analysis Date = 04/23/17 Pct Recovery = 70% Analysis Date = 04/23/17 Pct Recovery = 70% Analysis Date = 04/13/17 Pct Recovery = 70% Analysis Date = 04/13/17 Pct Recovery = 70% Analysis Date = 04/04/17 Pct Recovery = 70% Analysis Date = 04/04/17 Pct Recovery = 70% Analysis Date = 03/25/17 Pct Recovery = 69% Analysis Date = 03/25/17 Pct Recovery = 69% Analysis Date = 03/15/17 Pct Recovery = 69% Analysis Date = 03/15/17 Pct Recovery = 69% Analysis Date = 03/05/17 Pct Recovery = 69% Analysis Date = 03/05/17 Pct Recovery = 69% Analysis Date = 02/23/17 Pct Recovery = 69% Analysis Date = 02/23/17 Pct Recovery = 69% Analysis Date = 02/14/17 Pct Recovery = 69% Analysis Date = 02/14/17 Pct Recovery = 69% Analysis Date = 02/04/17 Pct Recovery = 69% Analysis Date = 02/04/17 Pct Recovery = 69% Analysis Date = 01/25/17 Pct Recovery = 69% Analysis Date = 01/25/17 Pct Recovery = 69% Analysis Date = 01/15/17 Pct Recovery = 69% Analysis Date = 01/15/17 Pct Recovery = 69% Analysis Date = 01/05/17 Pct Recovery = 69% Analysis Date = 01/05/17 Pct Recovery = 69% Analysis Date = 12/27/16 Pct Recovery = 68% Analysis Date = 12/27/16 Pct Recovery = 68% Analysis Date = 12/17/16 Pct Recovery = 68% Analysis Date = 12/17/16 Pct Recovery = 68% Analysis Date = 12/07/16 Pct Recovery = 68% Analysis Date = 12/07/16 Pct Recovery = 68% Analysis Date = 11/27/16 Pct Recovery = 68% Analysis Date = 11/27/16 Pct Recovery = 68% Analysis Date = 11/17/16 Pct Recovery = 68% Analysis Date = 11/17/16 Pct Recovery = 68% Analysis Date = 11/08/16 Pct Recovery = 68% Analysis Date = 11/08/16 Pct Recovery = 68% Analysis Date = 10/29/16 Pct Recovery = 68% Analysis Date = 10/29/16 Pct Recovery = 68% Analysis Date = 10/19/16 Pct Recovery = 68% Analysis Date = 10/19/16 Pct Recovery = 68% Analysis Date = 10/09/16 Pct Recovery = 68% Analysis Date = 10/09/16 Pct Recovery = 68% Analysis Date = 09/29/16 Pct Recovery = 68% Analysis Date = 09/29/16 Pct Recovery = 68% Analysis Date = 09/19/16 Pct Recovery = 68% Analysis Date = 09/19/16 Pct Recovery = 68% Analysis Date = 09/10/16 Pct Recovery = 68% Analysis Date = 09/10/16 Pct Recovery = 68% Analysis Date = 08/31/16 Pct Recovery = 68% Analysis Date = 08/31/16 Pct Recovery = 68% Analysis Date = 08/21/16 Pct Recovery = 68% Analysis Date = 08/21/16 Pct Recovery = 68% Analysis Date = 08/11/16 Pct Recovery = 68% Analysis Date = 08/11/16 Pct Recovery = 68% Analysis Date = 08/01/16 Pct Recovery = 68% Analysis Date = 08/01/16 Pct Recovery = 68% Analysis Date = 07/23/16 Pct Recovery = 68% Analysis Date = 07/23/16 Pct Recovery = 68% Analysis Date = 07/13/16 Pct Recovery = 68% Analysis Date = 07/13/16 Pct Recovery = 68% Analysis Date = 07/03/16 Pct Recovery = 68% Analysis Date = 07/03/16 Pct Recovery = 68% Analysis Date = 06/23/16 Pct Recovery = 68% Analysis Date = 06/23/16 Pct Recovery = 68% Analysis Date = 06/13/16 Pct Recovery = 68% Analysis Date = 06/13/16 Pct Recovery = 68% Analysis Date = 06/04/16 Pct Recovery = 68% Analysis Date = 06/04/16 Pct Recovery = 68% Analysis Date = 05/25/16 Pct Recovery = 68% Analysis Date = 05/25/16 Pct Recovery = 68% Analysis Date = 05/15/16 Pct Recovery = 68% Analysis Date = 05/15/16 Pct Recovery = 68% Analysis Date = 05/05/16 Pct Recovery = 68% Analysis Date = 05/05/16 Pct Recovery = 68% Analysis Date = 04/25/16 Pct Recovery = 68% Analysis Date = 04/25/16 Pct Recovery = 68% Analysis Date = 04/16/16 Pct Recovery = 68% Analysis Date = 04/16/16 Pct Recovery = 68% Analysis Date = 04/06/16 Pct Recovery = 68% Analysis Date = 04/06/16 Pct Recovery = 68% Analysis Date = 03/27/16 Pct Recovery = 68% Analysis Date = 03/27/16 Pct Recovery = 68% Analysis Date = 03/17/16 Pct Recovery = 68% Analysis Date = 03/17/16 Pct Recovery = 68% Analysis Date = 03/07/16 Pct Recovery = 68% Analysis Date = 03/07/16 Pct Recovery = 68% Analysis Date = 02/26/16 Pct Recovery = 68% Analysis Date = 02/26/16 Pct Recovery = 68% Analysis Date = 02/17/16 Pct Recovery = 68% Analysis Date = 02/17/16 Pct Recovery = 68% Analysis Date = 02/07/16 Pct Recovery = 68% Analysis Date = 02/07/16 Pct Recovery = 68% Analysis Date = 01/28/16 Pct Recovery = 68% Analysis Date = 01/28/16 Pct Recovery = 68% Analysis Date = 01/18/16 Pct Recovery = 68% Analysis Date = 01/18/16 Pct Recovery = 68% Analysis Date = 01/08/16 Pct Recovery = 68% Analysis Date = 01/08/16 Pct Recovery = 68% Analysis Date = 12/30/15 Pct Recovery = 67% Analysis Date = 12/30/15 Pct Recovery = 67% Analysis Date = 12/20/15 Pct Recovery = 67% Analysis Date = 12/20/15 Pct Recovery = 67% Analysis Date = 12/10/15 Pct Recovery = 67% Analysis Date = 12/10/15 Pct Recovery = 67% Analysis Date = 11/30/15 Pct Recovery = 67% Analysis Date = 11/30/15 Pct Recovery = 67% Analysis Date = 11/20/15 Pct Recovery = 67% Analysis Date = 11/20/15 Pct Recovery = 67% Analysis Date = 11/11/15 Pct Recovery = 67% Analysis Date = 11/11/15 Pct Recovery = 67% Analysis Date = 11/01/15 Pct Recovery = 66% Analysis Date = 11/01/15 Pct Recovery = 66% Analysis Date = 10/22/15 Pct Recovery = 66% Analysis Date = 10/22/15 Pct Recovery = 66% Analysis Date = 10/12/15 Pct Recovery = 66% Analysis Date = 10/12/15 Pct Recovery = 66% Analysis Date = 10/02/15 Pct Recovery = 66% Analysis Date = 10/02/15 Pct Recovery = 66% Analysis Date = 09/23/15 Pct Recovery = 66% Analysis Date = 09/23/15 Pct Recovery = 66% Analysis Date = 09/13/15 Pct Recovery = 66% Analysis Date = 09/13/15 Pct Recovery = 66% Analysis Date = 09/03/15 Pct Recovery = 66% Analysis Date = 09/03/15 Pct Recovery = 66% Analysis Date = 08/24/15 Pct Recovery = 65% Analysis Date = 08/24/15 Pct Recovery = 65% Analysis Date = 08/14/15 Pct Recovery = 65% Analysis Date = 08/14/15 Pct Recovery = 65% Analysis Date = 08/04/15 Pct Recovery = 65% Analysis Date = 08/04/15 Pct Recovery = 65% Analysis Date = 07/26/15 Pct Recovery = 65% Analysis Date = 07/26/15 Pct Recovery = 65% Analysis Date = 07/16/15 Pct Recovery = 65% Analysis Date = 07/16/15 Pct Recovery = 65% Analysis Date = 07/06/15 Pct Recovery = 65% Analysis Date = 07/06/15 Pct Recovery = 65% Analysis Date = 06/26/15 Pct Recovery = 64% Analysis Date = 06/26/15 Pct Recovery = 64% Analysis Date = 06/16/15 Pct Recovery = 64% Analysis Date = 06/16/15 Pct Recovery = 64% Analysis Date = 06/07/15 Pct Recovery = 64% Analysis Date = 06/07/15 Pct Recovery = 64% Analysis Date = 05/28/15 Pct Recovery = 64% Analysis Date = 05/28/15 Pct Recovery = 64% Analysis Date = 05/18/15 Pct Recovery = 64% Analysis Date = 05/18/15 Pct Recovery = 64% Analysis Date = 05/08/15 Pct Recovery = 64% Analysis Date = 05/08/15 Pct Recovery = 64% Analysis Date = 04/28/15 Pct Recovery = 63% Analysis Date = 04/28/15 Pct Recovery = 63% Analysis Date = 04/19/15 Pct Recovery = 63% Analysis Date = 04/19/15 Pct Recovery = 63% Analysis Date = 04/09/15 Pct Recovery = 63% Analysis Date = 04/09/15 Pct Recovery = 63% Analysis Date = 03/30/15 Pct Recovery = 63% Analysis Date = 03/30/15 Pct Recovery = 63% Analysis Date = 03/20/15 Pct Recovery = 63% Analysis Date = 03/20/15 Pct Recovery = 63% Analysis Date = 03/10/15 Pct Recovery = 63% Analysis Date = 03/10/15 Pct Recovery = 63% Analysis Date = 02/28/15 Pct Recovery = 62% Analysis Date = 02/28/15 Pct Recovery = 62% Analysis Date = 02/19/15 Pct Recovery = 62% Analysis Date = 02/19/15 Pct Recovery = 62% Analysis Date = 02/09/15 Pct Recovery = 62% Analysis Date = 02/09/15 Pct Recovery = 62% Analysis Date = 01/30/15 Pct Recovery = 62% Analysis Date = 01/30/15 Pct Recovery = 62% Analysis Date = 01/20/15 Pct Recovery = 62% Analysis Date = 01/20/15 Pct Recovery = 62% Analysis Date = 01/10/15 Pct Recovery = 62% Analysis Date = 01/10/15 Pct Recovery = 62% Analysis Date = 01/01/15 Pct Recovery = 62% Analysis Date = 01/01/15 Pct Recovery = 62% Analysis Date = 12/22/14 Pct Recovery = 61% Analysis Date = 12/22/14 Pct Recovery = 61% Analysis Date = 12/12/14 Pct Recovery = 61% Analysis Date = 12/12/14 Pct Recovery = 61% Analysis Date = 12/02/14 Pct Recovery = 61% Analysis Date = 12/02/14 Pct Recovery = 61% Analysis Date = 11/22/14 Pct Recovery = 61% Analysis Date = 11/22/14 Pct Recovery = 61% Analysis Date = 11/13/14 Pct Recovery = 61% Analysis Date = 11/13/14 Pct Recovery = 61% Analysis Date = 11/03/14 Pct Recovery = 60% Analysis Date = 11/03/14 Pct Recovery = 60% Analysis Date = 10/24/14 Pct Recovery = 60% Analysis Date = 10/24/14 Pct Recovery = 60% Analysis Date = 10/14/14 Pct Recovery = 60% Analysis Date = 10/14/14 Pct Recovery = 60% Analysis Date = 10/04/14 Pct Recovery = 59% Analysis Date = 10/04/14 Pct Recovery = 59% Analysis Date = 09/25/14 Pct Recovery = 59% Analysis Date = 09/25/14 Pct Recovery = 59% Analysis Date = 09/15/14 Pct Recovery = 59% Analysis Date = 09/15/14 Pct Recovery = 59% Analysis Date = 09/05/14 Pct Recovery = 58% Analysis Date = 09/05/14 Pct Recovery = 58% Analysis Date = 08/26/14 Pct Recovery = 58% Analysis Date = 08/26/14 Pct Recovery = 58% Analysis Date = 08/16/14 Pct Recovery = 58% Analysis Date = 08/16/14 Pct Recovery = 58% Analysis Date = 08/06/14 Pct Recovery = 57% Analysis Date = 08/06/14 Pct Recovery = 57% Analysis Date = 07/28/14 Pct Recovery = 57% Analysis Date = 07/28/14 Pct Recovery = 57% Analysis Date = 07/18/14 Pct Recovery = 57% Analysis Date = 07/18/14 Pct Recovery = 57% Analysis Date = 07/08/14 Pct Recovery = 57% Analysis Date = 07/08/14 Pct Recovery = 57% Analysis Date = 06/28/14 Pct Recovery = 56% Analysis Date = 06/28/14 Pct Recovery = 56% Analysis Date = 06/18/14 Pct Recovery = 56% Analysis Date = 06/18/14 Pct Recovery = 56% Analysis Date = 06/09/14 Pct Recovery = 56% Analysis Date = 06/09/14 Pct Recovery = 56% Analysis Date = 05/30/14 Pct Recovery = 56% Analysis Date = 05/30/14 Pct Recovery = 56% Analysis Date = 05/20/14 Pct Recovery = 55% Analysis Date = 05/20/14 Pct Recovery = 55% Analysis Date = 05/10/14 Pct Recovery = 55% Analysis Date = 05/10/14 Pct Recovery = 55% Analysis Date = 04/30/14 Pct Recovery = 55% Analysis Date = 04/30/14 Pct Recovery = 55% Analysis Date = 04/21/14 Pct Recovery = 55% Analysis Date = 04/21/14 Pct Recovery = 55% Analysis Date = 04/11/14 Pct Recovery = 55% Analysis Date = 04/11/14 Pct Recovery = 55% Analysis Date = 04/01/14 Pct Recovery = 54% Analysis Date = 04/01/14 Pct Recovery = 54% Analysis Date = 03/22/14 Pct Recovery = 54% Analysis Date = 03/22/14 Pct Recovery = 54% Analysis Date = 03/12/14 Pct Recovery = 54% Analysis Date = 03/12/14 Pct Recovery = 54% Analysis Date = 03/03/14 Pct Recovery = 54% Analysis Date = 03/03/14 Pct Recovery = 54% Analysis Date = 02/21/14 Pct Recovery = 53% Analysis Date = 02/21/14 Pct Recovery = 53% Analysis Date = 02/11/14 Pct Recovery = 53% Analysis Date = 02/11/14 Pct Recovery = 53% Analysis Date = 02/01/14 Pct Recovery = 53% Analysis Date = 02/01/14 Pct Recovery = 53% Analysis Date = 01/22/14 Pct Recovery = 53% Analysis Date = 01/22/14 Pct Recovery = 53% Analysis Date = 01/12/14 Pct Recovery = 53% Analysis Date = 01/12/14 Pct Recovery = 53% Analysis Date = 01/03/14 Pct Recovery = 52% Analysis Date = 01/03/14 Pct Recovery = 52% Analysis Date = 12/24/13 Pct Recovery = 52% Analysis Date = 12/24/13 Pct Recovery = 52% Analysis Date = 12/14/13 Pct Recovery = 52% Analysis Date = 12/14/13 Pct Recovery = 52% Analysis Date = 12/04/13 Pct Recovery = 52% Analysis Date = 12/04/13 Pct Recovery = 52% Analysis Date = 11/24/13 Pct Recovery = 52% Analysis Date = 11/24/13 Pct Recovery = 52% Analysis Date = 11/15/13 Pct Recovery = 51% Analysis Date = 11/15/13 Pct Recovery = 51% Analysis Date = 11/05/13 Pct Recovery = 51% Analysis Date = 11/05/13 Pct Recovery = 51% Analysis Date = 10/26/13 Pct Recovery = 51% Analysis Date = 10/26/13 Pct Recovery = 51% Analysis Date = 10/16/13 Pct Recovery = 51% Analysis Date = 10/16/13 Pct Recovery = 51% Analysis Date = 10/06/13 Pct Recovery = 51% Analysis Date = 10/06/13 Pct Recovery = 51% Analysis Date = 09/27/13 Pct Recovery = 50% Analysis Date = 09/27/13 Pct Recovery = 50% Analysis Date = 09/17/13 Pct Recovery = 50% Analysis Date = 09/17/13 Pct Recovery = 50% Analysis Date = 09/07/13 Pct Recovery = 50% Analysis Date = 09/07/13 Pct Recovery = 50% Analysis Date = 08/28/13 Pct Recovery = 50% Analysis Date = 08/28/13 Pct Recovery = 50% Analysis Date = 08/18/13 Pct Recovery = 50% Analysis Date = 08/18/13 Pct Recovery = 50% Analysis Date = 08/09/13 Pct Recovery = 50% Analysis Date = 08/09/13 Pct Recovery = 50% Analysis Date = 07/30/13 Pct Recovery = 49% Analysis Date = 07/30/13 Pct Recovery = 49% Analysis Date = 07/20/13 Pct Recovery = 49% Analysis Date = 07/20/13 Pct Recovery = 49% Analysis Date = 07/10/13 Pct Recovery = 49% Analysis Date = 07/10/13 Pct Recovery = 49% Analysis Date = 06/30/13 Pct Recovery = 49% Analysis Date = 06/30/13 Pct Recovery = 49% Analysis Date = 06/20/13 Pct Recovery = 49% Analysis Date = 06/20/13 Pct Recovery = 49% Analysis Date = 06/11/13 Pct Recovery = 49% Analysis Date = 06/11/13 Pct Recovery = 49% Analysis Date = 06/01/13 Pct Recovery = 48% Analysis Date = 06/01/13 Pct Recovery = 48% Analysis Date = 05/22/13 Pct Recovery = 48% Analysis Date = 05/22/13 Pct Recovery = 48% Analysis Date = 05/12/13 Pct Recovery = 48% Analysis Date = 05/12/13 Pct Recovery = 48% Analysis Date = 05/02/13 Pct Recovery = 48% Analysis Date = 05/02/13 Pct Recovery = 48% Analysis Date = 04/23/13 Pct Recovery = 48% Analysis Date = 04/23/13 Pct Recovery = 48% Analysis Date = 04/13/13 Pct Recovery = 48% Analysis Date = 04/13/13 Pct Recovery = 48% Analysis Date = 04/03/13 Pct Recovery = 48% Analysis Date = 04/03/13 Pct Recovery = 48% Analysis Date = 03/24/13 Pct Recovery = 47% Analysis Date = 03/24/13 Pct Recovery = 47% Analysis Date = 03/14/13 Pct Recovery = 47% Analysis Date = 03/14/13 Pct Recovery = 47% Analysis Date = 03/05/13 Pct Recovery = 47% Analysis Date = 03/05/13 Pct Recovery = 47% Analysis Date = 02/23/13 Pct Recovery = 47% Analysis Date = 02/23/13 Pct Recovery = 47% Analysis Date = 02/13/13 Pct Recovery = 47% Analysis Date = 02/13/13 Pct Recovery = 47% Analysis Date = 02/03/13 Pct Recovery = 47% Analysis Date = 02/03/13 Pct Recovery = 47% Analysis Date = 01/24/13 Pct Recovery = 47% Analysis Date = 01/24/13 Pct Recovery = 47% Analysis Date = 01/15/13 Pct Recovery = 46% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
HEXAZINONE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 77 62% 20% 63% 19%
Total 77 62% 20% 63% 19%

Sample Statistics
HEXAZINONE

Characteristic N % % Basis
Plotted 77 100% Spiked
Estimated Values 3 4% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 77 .  
False Negatives 0 0% 0 out of 77
Not Spiked 57 .  
False Positives 0 0% 0 out of 57

OBSP Determination:
IPRODIONE
METHOD: 2033 , TESTIDCODE: 61593GCM39

Laboratory ID = 20132490342 Lab Value = 0.148 Expected Conc. = 0.248 Report level label = 0.014 Pct Recovery = 60% Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20130940097 Lab Value = 0.100 Expected Conc. = 0.1255 Report level label = 0.014 Pct Recovery = 80% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = 0507-12-04.2 Laboratory ID = 20123560092 Lab Value = 0.084 Expected Conc. = 0.1255 Report level label = 0.014 Pct Recovery = 67% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = 0507-12-04.2 Laboratory ID = 20130810108 Lab Value = 0.081 Expected Conc. = 0.1252 Report level label = 0.014 Pct Recovery = 65% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl SpecificMix = LB92783 Laboratory ID = 20130100066 Lab Value = 0.123 Expected Conc. = 0.1252 Report level label = 0.014 Pct Recovery = 98% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl SpecificMix = LB92783 Laboratory ID = 20132140002 Lab Value = 0.104 Expected Conc. = 0.125 Report level label = 0.014 Pct Recovery = 83% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl SpecificMix = LB99392 Laboratory ID = 20131370001 Lab Value = 0.114 Expected Conc. = 0.125 Report level label = 0.014 Pct Recovery = 91% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl SpecificMix = LB99392 Laboratory ID = 20140370077 Lab Value = 0.060 Expected Conc. = 0.124 Report level label = 0.014 Pct Recovery = 49% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20132560001 Lab Value = 0.100 Expected Conc. = 0.124 Report level label = 0.014 Pct Recovery = 81% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20180390003 Lab Value = 0.067 Expected Conc. = 0.093 Report level label = 0.014 Pct Recovery = 72% Analysis Date = 04/06/18 SpikeMix = Spex Organics EN170808006: 100 µl & Abs 071717Pest: 100 µl SpecificMix = 071717Pest Laboratory ID = 20172510330 Lab Value = 0.106 Expected Conc. = 0.093 Report level label = 0.014 Pct Recovery = 114% Analysis Date = 12/29/17 SpikeMix = ChemService 6537100: 100 µl & Abs 071817Pest: 100 µl SpecificMix = 6537100 Laboratory ID = 20163370001 Lab Value = 0.083 Expected Conc. = 0.0871 Report level label = 0.014 Pct Recovery = 96% Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl SpecificMix = B20160331 Laboratory ID = 20163150006 Lab Value = 0.080 Expected Conc. = 0.0871 Report level label = 0.014 Pct Recovery = 92% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl SpecificMix = B20160331 Laboratory ID = 20161880109 Lab Value = 0.098 Expected Conc. = 0.087 Report level label = 0.014 Pct Recovery = 112% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl SpecificMix = 03FF076 Laboratory ID = 20152610011 Lab Value = 0.081 Expected Conc. = 0.0832 Report level label = 0.014 Pct Recovery = 97% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl SpecificMix = 0406-15-01 Laboratory ID = 20152460215 Lab Value = 0.071 Expected Conc. = 0.0832 Report level label = 0.014 Pct Recovery = 86% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl SpecificMix = 0406-15-01 Laboratory ID = 20172020035 Lab Value = 0.072 Expected Conc. = 0.072 Report level label = 0.014 Pct Recovery = 100% Analysis Date = 11/07/17 SpikeMix = Abs 071717Pest: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20171720140 Lab Value = 0.071 Expected Conc. = 0.0697 Report level label = 0.014 Pct Recovery = 101% Analysis Date = 08/31/17 SpikeMix = Supelco LC20138V: 80 µl & Phenova B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20171660002 Lab Value = 0.077 Expected Conc. = 0.0697 Report level label = 0.014 Pct Recovery = 110% Analysis Date = 08/23/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20170190026 Lab Value = 0.067 Expected Conc. = 0.0697 Report level label = 0.014 Pct Recovery = 96% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20161470001 Lab Value = 0.070 Expected Conc. = 0.0697 Report level label = 0.014 Pct Recovery = 100% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20170960001 Lab Value = 0.065 Expected Conc. = 0.0696 Report level label = 0.014 Pct Recovery = 93% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl SpecificMix = 03FF076 Laboratory ID = 20143240095 Lab Value = 0.065 Expected Conc. = 0.0558 Report level label = 0.014 Pct Recovery = 117% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl SpecificMix = 032714 Laboratory ID = 20142270001 Lab Value = 0.034 Expected Conc. = 0.0558 Report level label = 0.014 Pct Recovery = 61% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl SpecificMix = 032714 Laboratory ID = 20141220025 Lab Value = 0.045 Expected Conc. = 0.0558 Report level label = 0.014 Pct Recovery = 81% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl SpecificMix = 032714 Laboratory ID = 20130510051 Lab Value = 0.047 Expected Conc. = 0.0502 Report level label = 0.014 Pct Recovery = 94% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl SpecificMix = 0507-12-04.2 Laboratory ID = 20130390105 Lab Value = 0.028 Expected Conc. = 0.0501 Report level label = 0.014 Pct Recovery = 56% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl SpecificMix = LB92783 Laboratory ID = 20140510043 Lab Value = 0.042 Expected Conc. = 0.05 Report level label = 0.014 Pct Recovery = 84% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl SpecificMix = LB99392 Laboratory ID = 20133470008 Lab Value = 0.042 Expected Conc. = 0.05 Report level label = 0.014 Pct Recovery = 84% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl SpecificMix = LB99392 Laboratory ID = 20133190012 Lab Value = 0.061 Expected Conc. = 0.05 Report level label = 0.014 Pct Recovery = 122% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = LB99392 Laboratory ID = 20133050050 Lab Value = 0.056 Expected Conc. = 0.05 Report level label = 0.014 Pct Recovery = 111% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl SpecificMix = LB99392 Laboratory ID = 20133580036 Lab Value = 0.041 Expected Conc. = 0.0496 Report level label = 0.014 Pct Recovery = 82% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20131790009 Lab Value = 0.034 Expected Conc. = 0.0496 Report level label = 0.014 Pct Recovery = 68% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20131510026 Lab Value = 0.048 Expected Conc. = 0.0496 Report level label = 0.014 Pct Recovery = 97% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20173480003 Lab Value = 0.040 Expected Conc. = 0.0465 Report level label = 0.014 Pct Recovery = 85% Analysis Date = 04/05/18 SpikeMix = Abs 071717Pest: 50 µl & ChemService 6567600: 50 µl SpecificMix = 071717Pest Laboratory ID = 20172370001 Lab Value = 0.052 Expected Conc. = 0.0465 Report level label = 0.014 Pct Recovery = 112% Analysis Date = 11/18/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6537100: 50 µl SpecificMix = 6537100 Laboratory ID = 20172230001 Lab Value = 0.049 Expected Conc. = 0.0465 Report level label = 0.014 Pct Recovery = 104% Analysis Date = 10/19/17 SpikeMix = ChemService 6472100: 50 µl & Abs 071717Pest: 50 µl SpecificMix = 071717Pest Laboratory ID = 20161260151 Lab Value = 0.033 Expected Conc. = 0.044 Report level label = 0.014 Pct Recovery = 76% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = 3851600 Laboratory ID = 20151550293 Lab Value = 0.042 Expected Conc. = 0.044 Report level label = 0.014 Pct Recovery = 94% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl SpecificMix = 3851600 Laboratory ID = 20151270112 Lab Value = 0.050 Expected Conc. = 0.044 Report level label = 0.014 Pct Recovery = 114% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl SpecificMix = 3851600 Laboratory ID = 20160770090 Lab Value = 0.038 Expected Conc. = 0.0416 Report level label = 0.014 Pct Recovery = 92% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20160630046 Lab Value = 0.031 Expected Conc. = 0.0416 Report level label = 0.014 Pct Recovery = 75% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20153510109 Lab Value = 0.038 Expected Conc. = 0.0416 Report level label = 0.014 Pct Recovery = 91% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20153440001 Lab Value = 0.036 Expected Conc. = 0.0416 Report level label = 0.014 Pct Recovery = 86% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20171160110 Lab Value = 0.039 Expected Conc. = 0.0348 Report level label = 0.014 Pct Recovery = 112% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = B20160331 Laboratory ID = 20162380004 Lab Value = 0.031 Expected Conc. = 0.0348 Report level label = 0.014 Pct Recovery = 90% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = B20160331 Laboratory ID = 20162150213 Lab Value = 0.037 Expected Conc. = 0.0348 Report level label = 0.014 Pct Recovery = 105% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl SpecificMix = B20160331 Laboratory ID = 20171510080 Lab Value = 0.036 Expected Conc. = 0.0348 Report level label = 0.014 Pct Recovery = 103% Analysis Date = 06/09/17 SpikeMix = Supelco LC20138V: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20170460061 Lab Value = 0.028 Expected Conc. = 0.0348 Report level label = 0.014 Pct Recovery = 82% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl SpecificMix = 03FF076 Laboratory ID = 20162660005 Lab Value = 0.034 Expected Conc. = 0.0348 Report level label = 0.014 Pct Recovery = 97% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl SpecificMix = 03FF076 Laboratory ID = 20161600087 Lab Value = 0.032 Expected Conc. = 0.0348 Report level label = 0.014 Pct Recovery = 92% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20161340228 Lab Value = 0.032 Expected Conc. = 0.0348 Report level label = 0.014 Pct Recovery = 93% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl SpecificMix = 03FF076 Laboratory ID = 20161190075 Lab Value = 0.030 Expected Conc. = 0.0348 Report level label = 0.014 Pct Recovery = 86% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20180940080 Lab Value = 0.034 Expected Conc. = 0.0279 Report level label = 0.014 Pct Recovery = 122% Analysis Date = 05/31/18 SpikeMix = ChemService 6472100: 30 µl & Abs 071717Pest: 30 µl SpecificMix = 071717Pest Laboratory ID = 20180730064 Lab Value = 0.034 Expected Conc. = 0.0279 Report level label = 0.014 Pct Recovery = 123% Analysis Date = 05/16/18 SpikeMix = Abs 071717Pest: 30 µl & Abs 071817Pest: 30 µl SpecificMix = 071717Pest Laboratory ID = 20173120093 Lab Value = 0.031 Expected Conc. = 0.0279 Report level label = 0.014 Pct Recovery = 113% Analysis Date = 03/10/18 SpikeMix = ChemService 6472100: 30 µl & ChemService 6537100: 30 µl SpecificMix = 6537100 Laboratory ID = 20172780018 Lab Value = 0.035 Expected Conc. = 0.0279 Report level label = 0.014 Pct Recovery = 124% Analysis Date = 02/08/18 SpikeMix = ChemService 6537100: 30 µl & Abs 071817Pest: 30 µl SpecificMix = 6537100 Laboratory ID = 20150150115 Lab Value = 0.025 Expected Conc. = 0.0279 Report level label = 0.014 Pct Recovery = 88% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl SpecificMix = 032714 Laboratory ID = 20142820151 Lab Value = 0.032 Expected Conc. = 0.0279 Report level label = 0.014 Pct Recovery = 113% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl SpecificMix = 032714 Laboratory ID = 20141490205 Lab Value = 0.027 Expected Conc. = 0.0279 Report level label = 0.014 Pct Recovery = 96% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = 032714 Laboratory ID = 20141080004 Lab Value = 0.019 Expected Conc. = 0.0279 Report level label = 0.014 Pct Recovery = 68% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl SpecificMix = 032714 Laboratory ID = 20160430111 Lab Value = 0.020 Expected Conc. = 0.022 Report level label = 0.014 Pct Recovery = 91% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 3851600 Laboratory ID = 20160210080 Lab Value = 0.016 Expected Conc. = 0.022 Report level label = 0.014 Pct Recovery = 71% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 3851600 Laboratory ID = 20152950078 Lab Value = 0.013 Expected Conc. = 0.022 Report level label = 0.014 Pct Recovery = 59% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 3851600 Laboratory ID = 20153030068 Lab Value = 0.018 Expected Conc. = 0.022 Report level label = 0.014 Pct Recovery = 83% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = 3851600 Laboratory ID = 20151760208 Lab Value = 0.028 Expected Conc. = 0.022 Report level label = 0.014 Pct Recovery = 126% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl SpecificMix = 3851600 Laboratory ID = 20151380009 Lab Value = 0.023 Expected Conc. = 0.022 Report level label = 0.014 Pct Recovery = 105% Analysis Date = 05/30/15 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 3851600 Laboratory ID = 20152190003 Lab Value = 0.020 Expected Conc. = 0.0208 Report level label = 0.014 Pct Recovery = 98% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = 0406-15-01 Laboratory ID = 20152040177 Lab Value = 0.026 Expected Conc. = 0.0208 Report level label = 0.014 Pct Recovery = 123% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl SpecificMix = 0406-15-01 Analysis Date = 05/31/18 Pct Recovery = 110% Analysis Date = 05/21/18 Pct Recovery = 110% Analysis Date = 05/21/18 Pct Recovery = 110% Analysis Date = 05/11/18 Pct Recovery = 109% Analysis Date = 05/11/18 Pct Recovery = 109% Analysis Date = 05/01/18 Pct Recovery = 109% Analysis Date = 05/01/18 Pct Recovery = 109% Analysis Date = 04/21/18 Pct Recovery = 109% Analysis Date = 04/21/18 Pct Recovery = 109% Analysis Date = 04/11/18 Pct Recovery = 109% Analysis Date = 04/11/18 Pct Recovery = 109% Analysis Date = 04/02/18 Pct Recovery = 108% Analysis Date = 04/02/18 Pct Recovery = 108% Analysis Date = 03/23/18 Pct Recovery = 108% Analysis Date = 03/23/18 Pct Recovery = 108% Analysis Date = 03/13/18 Pct Recovery = 108% Analysis Date = 03/13/18 Pct Recovery = 108% Analysis Date = 03/03/18 Pct Recovery = 107% Analysis Date = 03/03/18 Pct Recovery = 107% Analysis Date = 02/21/18 Pct Recovery = 107% Analysis Date = 02/21/18 Pct Recovery = 107% Analysis Date = 02/12/18 Pct Recovery = 107% Analysis Date = 02/12/18 Pct Recovery = 107% Analysis Date = 02/02/18 Pct Recovery = 107% Analysis Date = 02/02/18 Pct Recovery = 107% Analysis Date = 01/23/18 Pct Recovery = 106% Analysis Date = 01/23/18 Pct Recovery = 106% Analysis Date = 01/13/18 Pct Recovery = 106% Analysis Date = 01/13/18 Pct Recovery = 106% Analysis Date = 01/03/18 Pct Recovery = 106% Analysis Date = 01/03/18 Pct Recovery = 106% Analysis Date = 12/25/17 Pct Recovery = 106% Analysis Date = 12/25/17 Pct Recovery = 106% Analysis Date = 12/15/17 Pct Recovery = 105% Analysis Date = 12/15/17 Pct Recovery = 105% Analysis Date = 12/05/17 Pct Recovery = 105% Analysis Date = 12/05/17 Pct Recovery = 105% Analysis Date = 11/25/17 Pct Recovery = 105% Analysis Date = 11/25/17 Pct Recovery = 105% Analysis Date = 11/15/17 Pct Recovery = 105% Analysis Date = 11/15/17 Pct Recovery = 105% Analysis Date = 11/05/17 Pct Recovery = 104% Analysis Date = 11/05/17 Pct Recovery = 104% Analysis Date = 10/27/17 Pct Recovery = 104% Analysis Date = 10/27/17 Pct Recovery = 104% Analysis Date = 10/17/17 Pct Recovery = 104% Analysis Date = 10/17/17 Pct Recovery = 104% Analysis Date = 10/07/17 Pct Recovery = 103% Analysis Date = 10/07/17 Pct Recovery = 103% Analysis Date = 09/27/17 Pct Recovery = 103% Analysis Date = 09/27/17 Pct Recovery = 103% Analysis Date = 09/17/17 Pct Recovery = 103% Analysis Date = 09/17/17 Pct Recovery = 103% Analysis Date = 09/08/17 Pct Recovery = 103% Analysis Date = 09/08/17 Pct Recovery = 103% Analysis Date = 08/29/17 Pct Recovery = 102% Analysis Date = 08/29/17 Pct Recovery = 102% Analysis Date = 08/19/17 Pct Recovery = 102% Analysis Date = 08/19/17 Pct Recovery = 102% Analysis Date = 08/09/17 Pct Recovery = 102% Analysis Date = 08/09/17 Pct Recovery = 102% Analysis Date = 07/30/17 Pct Recovery = 102% Analysis Date = 07/30/17 Pct Recovery = 102% Analysis Date = 07/21/17 Pct Recovery = 101% Analysis Date = 07/21/17 Pct Recovery = 101% Analysis Date = 07/11/17 Pct Recovery = 101% Analysis Date = 07/11/17 Pct Recovery = 101% Analysis Date = 07/01/17 Pct Recovery = 101% Analysis Date = 07/01/17 Pct Recovery = 101% Analysis Date = 06/21/17 Pct Recovery = 100% Analysis Date = 06/21/17 Pct Recovery = 100% Analysis Date = 06/11/17 Pct Recovery = 100% Analysis Date = 06/11/17 Pct Recovery = 100% Analysis Date = 06/02/17 Pct Recovery = 100% Analysis Date = 06/02/17 Pct Recovery = 100% Analysis Date = 05/23/17 Pct Recovery = 100% Analysis Date = 05/23/17 Pct Recovery = 100% Analysis Date = 05/13/17 Pct Recovery = 99% Analysis Date = 05/13/17 Pct Recovery = 99% Analysis Date = 05/03/17 Pct Recovery = 99% Analysis Date = 05/03/17 Pct Recovery = 99% Analysis Date = 04/23/17 Pct Recovery = 99% Analysis Date = 04/23/17 Pct Recovery = 99% Analysis Date = 04/13/17 Pct Recovery = 99% Analysis Date = 04/13/17 Pct Recovery = 99% Analysis Date = 04/04/17 Pct Recovery = 98% Analysis Date = 04/04/17 Pct Recovery = 98% Analysis Date = 03/25/17 Pct Recovery = 98% Analysis Date = 03/25/17 Pct Recovery = 98% Analysis Date = 03/15/17 Pct Recovery = 98% Analysis Date = 03/15/17 Pct Recovery = 98% Analysis Date = 03/05/17 Pct Recovery = 97% Analysis Date = 03/05/17 Pct Recovery = 97% Analysis Date = 02/23/17 Pct Recovery = 97% Analysis Date = 02/23/17 Pct Recovery = 97% Analysis Date = 02/14/17 Pct Recovery = 97% Analysis Date = 02/14/17 Pct Recovery = 97% Analysis Date = 02/04/17 Pct Recovery = 97% Analysis Date = 02/04/17 Pct Recovery = 97% Analysis Date = 01/25/17 Pct Recovery = 97% Analysis Date = 01/25/17 Pct Recovery = 97% Analysis Date = 01/15/17 Pct Recovery = 96% Analysis Date = 01/15/17 Pct Recovery = 96% Analysis Date = 01/05/17 Pct Recovery = 96% Analysis Date = 01/05/17 Pct Recovery = 96% Analysis Date = 12/27/16 Pct Recovery = 96% Analysis Date = 12/27/16 Pct Recovery = 96% Analysis Date = 12/17/16 Pct Recovery = 96% Analysis Date = 12/17/16 Pct Recovery = 96% Analysis Date = 12/07/16 Pct Recovery = 96% Analysis Date = 12/07/16 Pct Recovery = 96% Analysis Date = 11/27/16 Pct Recovery = 96% Analysis Date = 11/27/16 Pct Recovery = 96% Analysis Date = 11/17/16 Pct Recovery = 95% Analysis Date = 11/17/16 Pct Recovery = 95% Analysis Date = 11/08/16 Pct Recovery = 95% Analysis Date = 11/08/16 Pct Recovery = 95% Analysis Date = 10/29/16 Pct Recovery = 95% Analysis Date = 10/29/16 Pct Recovery = 95% Analysis Date = 10/19/16 Pct Recovery = 95% Analysis Date = 10/19/16 Pct Recovery = 95% Analysis Date = 10/09/16 Pct Recovery = 95% Analysis Date = 10/09/16 Pct Recovery = 95% Analysis Date = 09/29/16 Pct Recovery = 95% Analysis Date = 09/29/16 Pct Recovery = 95% Analysis Date = 09/19/16 Pct Recovery = 94% Analysis Date = 09/19/16 Pct Recovery = 94% Analysis Date = 09/10/16 Pct Recovery = 94% Analysis Date = 09/10/16 Pct Recovery = 94% Analysis Date = 08/31/16 Pct Recovery = 94% Analysis Date = 08/31/16 Pct Recovery = 94% Analysis Date = 08/21/16 Pct Recovery = 94% Analysis Date = 08/21/16 Pct Recovery = 94% Analysis Date = 08/11/16 Pct Recovery = 94% Analysis Date = 08/11/16 Pct Recovery = 94% Analysis Date = 08/01/16 Pct Recovery = 94% Analysis Date = 08/01/16 Pct Recovery = 94% Analysis Date = 07/23/16 Pct Recovery = 93% Analysis Date = 07/23/16 Pct Recovery = 93% Analysis Date = 07/13/16 Pct Recovery = 93% Analysis Date = 07/13/16 Pct Recovery = 93% Analysis Date = 07/03/16 Pct Recovery = 93% Analysis Date = 07/03/16 Pct Recovery = 93% Analysis Date = 06/23/16 Pct Recovery = 93% Analysis Date = 06/23/16 Pct Recovery = 93% Analysis Date = 06/13/16 Pct Recovery = 93% Analysis Date = 06/13/16 Pct Recovery = 93% Analysis Date = 06/04/16 Pct Recovery = 93% Analysis Date = 06/04/16 Pct Recovery = 93% Analysis Date = 05/25/16 Pct Recovery = 93% Analysis Date = 05/25/16 Pct Recovery = 93% Analysis Date = 05/15/16 Pct Recovery = 93% Analysis Date = 05/15/16 Pct Recovery = 93% Analysis Date = 05/05/16 Pct Recovery = 93% Analysis Date = 05/05/16 Pct Recovery = 93% Analysis Date = 04/25/16 Pct Recovery = 93% Analysis Date = 04/25/16 Pct Recovery = 93% Analysis Date = 04/16/16 Pct Recovery = 93% Analysis Date = 04/16/16 Pct Recovery = 93% Analysis Date = 04/06/16 Pct Recovery = 93% Analysis Date = 04/06/16 Pct Recovery = 93% Analysis Date = 03/27/16 Pct Recovery = 93% Analysis Date = 03/27/16 Pct Recovery = 93% Analysis Date = 03/17/16 Pct Recovery = 93% Analysis Date = 03/17/16 Pct Recovery = 93% Analysis Date = 03/07/16 Pct Recovery = 93% Analysis Date = 03/07/16 Pct Recovery = 93% Analysis Date = 02/26/16 Pct Recovery = 94% Analysis Date = 02/26/16 Pct Recovery = 94% Analysis Date = 02/17/16 Pct Recovery = 94% Analysis Date = 02/17/16 Pct Recovery = 94% Analysis Date = 02/07/16 Pct Recovery = 94% Analysis Date = 02/07/16 Pct Recovery = 94% Analysis Date = 01/28/16 Pct Recovery = 94% Analysis Date = 01/28/16 Pct Recovery = 94% Analysis Date = 01/18/16 Pct Recovery = 94% Analysis Date = 01/18/16 Pct Recovery = 94% Analysis Date = 01/08/16 Pct Recovery = 94% Analysis Date = 01/08/16 Pct Recovery = 94% Analysis Date = 12/30/15 Pct Recovery = 94% Analysis Date = 12/30/15 Pct Recovery = 94% Analysis Date = 12/20/15 Pct Recovery = 94% Analysis Date = 12/20/15 Pct Recovery = 94% Analysis Date = 12/10/15 Pct Recovery = 94% Analysis Date = 12/10/15 Pct Recovery = 94% Analysis Date = 11/30/15 Pct Recovery = 94% Analysis Date = 11/30/15 Pct Recovery = 94% Analysis Date = 11/20/15 Pct Recovery = 94% Analysis Date = 11/20/15 Pct Recovery = 94% Analysis Date = 11/11/15 Pct Recovery = 94% Analysis Date = 11/11/15 Pct Recovery = 94% Analysis Date = 11/01/15 Pct Recovery = 94% Analysis Date = 11/01/15 Pct Recovery = 94% Analysis Date = 10/22/15 Pct Recovery = 94% Analysis Date = 10/22/15 Pct Recovery = 94% Analysis Date = 10/12/15 Pct Recovery = 94% Analysis Date = 10/12/15 Pct Recovery = 94% Analysis Date = 10/02/15 Pct Recovery = 94% Analysis Date = 10/02/15 Pct Recovery = 94% Analysis Date = 09/23/15 Pct Recovery = 94% Analysis Date = 09/23/15 Pct Recovery = 94% Analysis Date = 09/13/15 Pct Recovery = 94% Analysis Date = 09/13/15 Pct Recovery = 94% Analysis Date = 09/03/15 Pct Recovery = 94% Analysis Date = 09/03/15 Pct Recovery = 94% Analysis Date = 08/24/15 Pct Recovery = 94% Analysis Date = 08/24/15 Pct Recovery = 94% Analysis Date = 08/14/15 Pct Recovery = 94% Analysis Date = 08/14/15 Pct Recovery = 94% Analysis Date = 08/04/15 Pct Recovery = 94% Analysis Date = 08/04/15 Pct Recovery = 94% Analysis Date = 07/26/15 Pct Recovery = 94% Analysis Date = 07/26/15 Pct Recovery = 94% Analysis Date = 07/16/15 Pct Recovery = 94% Analysis Date = 07/16/15 Pct Recovery = 94% Analysis Date = 07/06/15 Pct Recovery = 94% Analysis Date = 07/06/15 Pct Recovery = 94% Analysis Date = 06/26/15 Pct Recovery = 94% Analysis Date = 06/26/15 Pct Recovery = 94% Analysis Date = 06/16/15 Pct Recovery = 94% Analysis Date = 06/16/15 Pct Recovery = 94% Analysis Date = 06/07/15 Pct Recovery = 94% Analysis Date = 06/07/15 Pct Recovery = 94% Analysis Date = 05/28/15 Pct Recovery = 94% Analysis Date = 05/28/15 Pct Recovery = 94% Analysis Date = 05/18/15 Pct Recovery = 93% Analysis Date = 05/18/15 Pct Recovery = 93% Analysis Date = 05/08/15 Pct Recovery = 93% Analysis Date = 05/08/15 Pct Recovery = 93% Analysis Date = 04/28/15 Pct Recovery = 93% Analysis Date = 04/28/15 Pct Recovery = 93% Analysis Date = 04/19/15 Pct Recovery = 93% Analysis Date = 04/19/15 Pct Recovery = 93% Analysis Date = 04/09/15 Pct Recovery = 93% Analysis Date = 04/09/15 Pct Recovery = 93% Analysis Date = 03/30/15 Pct Recovery = 93% Analysis Date = 03/30/15 Pct Recovery = 93% Analysis Date = 03/20/15 Pct Recovery = 93% Analysis Date = 03/20/15 Pct Recovery = 93% Analysis Date = 03/10/15 Pct Recovery = 93% Analysis Date = 03/10/15 Pct Recovery = 93% Analysis Date = 02/28/15 Pct Recovery = 93% Analysis Date = 02/28/15 Pct Recovery = 93% Analysis Date = 02/19/15 Pct Recovery = 93% Analysis Date = 02/19/15 Pct Recovery = 93% Analysis Date = 02/09/15 Pct Recovery = 93% Analysis Date = 02/09/15 Pct Recovery = 93% Analysis Date = 01/30/15 Pct Recovery = 93% Analysis Date = 01/30/15 Pct Recovery = 93% Analysis Date = 01/20/15 Pct Recovery = 93% Analysis Date = 01/20/15 Pct Recovery = 93% Analysis Date = 01/10/15 Pct Recovery = 93% Analysis Date = 01/10/15 Pct Recovery = 93% Analysis Date = 01/01/15 Pct Recovery = 93% Analysis Date = 01/01/15 Pct Recovery = 93% Analysis Date = 12/22/14 Pct Recovery = 93% Analysis Date = 12/22/14 Pct Recovery = 93% Analysis Date = 12/12/14 Pct Recovery = 93% Analysis Date = 12/12/14 Pct Recovery = 93% Analysis Date = 12/02/14 Pct Recovery = 93% Analysis Date = 12/02/14 Pct Recovery = 93% Analysis Date = 11/22/14 Pct Recovery = 93% Analysis Date = 11/22/14 Pct Recovery = 93% Analysis Date = 11/13/14 Pct Recovery = 93% Analysis Date = 11/13/14 Pct Recovery = 93% Analysis Date = 11/03/14 Pct Recovery = 93% Analysis Date = 11/03/14 Pct Recovery = 93% Analysis Date = 10/24/14 Pct Recovery = 93% Analysis Date = 10/24/14 Pct Recovery = 93% Analysis Date = 10/14/14 Pct Recovery = 93% Analysis Date = 10/14/14 Pct Recovery = 93% Analysis Date = 10/04/14 Pct Recovery = 92% Analysis Date = 10/04/14 Pct Recovery = 92% Analysis Date = 09/25/14 Pct Recovery = 92% Analysis Date = 09/25/14 Pct Recovery = 92% Analysis Date = 09/15/14 Pct Recovery = 92% Analysis Date = 09/15/14 Pct Recovery = 92% Analysis Date = 09/05/14 Pct Recovery = 92% Analysis Date = 09/05/14 Pct Recovery = 92% Analysis Date = 08/26/14 Pct Recovery = 91% Analysis Date = 08/26/14 Pct Recovery = 91% Analysis Date = 08/16/14 Pct Recovery = 91% Analysis Date = 08/16/14 Pct Recovery = 91% Analysis Date = 08/06/14 Pct Recovery = 91% Analysis Date = 08/06/14 Pct Recovery = 91% Analysis Date = 07/28/14 Pct Recovery = 91% Analysis Date = 07/28/14 Pct Recovery = 91% Analysis Date = 07/18/14 Pct Recovery = 91% Analysis Date = 07/18/14 Pct Recovery = 91% Analysis Date = 07/08/14 Pct Recovery = 90% Analysis Date = 07/08/14 Pct Recovery = 90% Analysis Date = 06/28/14 Pct Recovery = 90% Analysis Date = 06/28/14 Pct Recovery = 90% Analysis Date = 06/18/14 Pct Recovery = 90% Analysis Date = 06/18/14 Pct Recovery = 90% Analysis Date = 06/09/14 Pct Recovery = 90% Analysis Date = 06/09/14 Pct Recovery = 90% Analysis Date = 05/30/14 Pct Recovery = 89% Analysis Date = 05/30/14 Pct Recovery = 89% Analysis Date = 05/20/14 Pct Recovery = 89% Analysis Date = 05/20/14 Pct Recovery = 89% Analysis Date = 05/10/14 Pct Recovery = 89% Analysis Date = 05/10/14 Pct Recovery = 89% Analysis Date = 04/30/14 Pct Recovery = 89% Analysis Date = 04/30/14 Pct Recovery = 89% Analysis Date = 04/21/14 Pct Recovery = 88% Analysis Date = 04/21/14 Pct Recovery = 88% Analysis Date = 04/11/14 Pct Recovery = 88% Analysis Date = 04/11/14 Pct Recovery = 88% Analysis Date = 04/01/14 Pct Recovery = 88% Analysis Date = 04/01/14 Pct Recovery = 88% Analysis Date = 03/22/14 Pct Recovery = 88% Analysis Date = 03/22/14 Pct Recovery = 88% Analysis Date = 03/12/14 Pct Recovery = 87% Analysis Date = 03/12/14 Pct Recovery = 87% Analysis Date = 03/03/14 Pct Recovery = 87% Analysis Date = 03/03/14 Pct Recovery = 87% Analysis Date = 02/21/14 Pct Recovery = 87% Analysis Date = 02/21/14 Pct Recovery = 87% Analysis Date = 02/11/14 Pct Recovery = 87% Analysis Date = 02/11/14 Pct Recovery = 87% Analysis Date = 02/01/14 Pct Recovery = 86% Analysis Date = 02/01/14 Pct Recovery = 86% Analysis Date = 01/22/14 Pct Recovery = 86% Analysis Date = 01/22/14 Pct Recovery = 86% Analysis Date = 01/12/14 Pct Recovery = 86% Analysis Date = 01/12/14 Pct Recovery = 86% Analysis Date = 01/03/14 Pct Recovery = 86% Analysis Date = 01/03/14 Pct Recovery = 86% Analysis Date = 12/24/13 Pct Recovery = 85% Analysis Date = 12/24/13 Pct Recovery = 85% Analysis Date = 12/14/13 Pct Recovery = 85% Analysis Date = 12/14/13 Pct Recovery = 85% Analysis Date = 12/04/13 Pct Recovery = 85% Analysis Date = 12/04/13 Pct Recovery = 85% Analysis Date = 11/24/13 Pct Recovery = 84% Analysis Date = 11/24/13 Pct Recovery = 84% Analysis Date = 11/15/13 Pct Recovery = 84% Analysis Date = 11/15/13 Pct Recovery = 84% Analysis Date = 11/05/13 Pct Recovery = 84% Analysis Date = 11/05/13 Pct Recovery = 84% Analysis Date = 10/26/13 Pct Recovery = 84% Analysis Date = 10/26/13 Pct Recovery = 84% Analysis Date = 10/16/13 Pct Recovery = 83% Analysis Date = 10/16/13 Pct Recovery = 83% Analysis Date = 10/06/13 Pct Recovery = 83% Analysis Date = 10/06/13 Pct Recovery = 83% Analysis Date = 09/27/13 Pct Recovery = 83% Analysis Date = 09/27/13 Pct Recovery = 83% Analysis Date = 09/17/13 Pct Recovery = 83% Analysis Date = 09/17/13 Pct Recovery = 83% Analysis Date = 09/07/13 Pct Recovery = 82% Analysis Date = 09/07/13 Pct Recovery = 82% Analysis Date = 08/28/13 Pct Recovery = 82% Analysis Date = 08/28/13 Pct Recovery = 82% Analysis Date = 08/18/13 Pct Recovery = 82% Analysis Date = 08/18/13 Pct Recovery = 82% Analysis Date = 08/09/13 Pct Recovery = 82% Analysis Date = 08/09/13 Pct Recovery = 82% Analysis Date = 07/30/13 Pct Recovery = 81% Analysis Date = 07/30/13 Pct Recovery = 81% Analysis Date = 07/20/13 Pct Recovery = 81% Analysis Date = 07/20/13 Pct Recovery = 81% Analysis Date = 07/10/13 Pct Recovery = 81% Analysis Date = 07/10/13 Pct Recovery = 81% Analysis Date = 06/30/13 Pct Recovery = 80% Analysis Date = 06/30/13 Pct Recovery = 80% Analysis Date = 06/20/13 Pct Recovery = 80% Analysis Date = 06/20/13 Pct Recovery = 80% Analysis Date = 06/11/13 Pct Recovery = 80% Analysis Date = 06/11/13 Pct Recovery = 80% Analysis Date = 06/01/13 Pct Recovery = 80% Analysis Date = 06/01/13 Pct Recovery = 80% Analysis Date = 05/22/13 Pct Recovery = 79% Analysis Date = 05/22/13 Pct Recovery = 79% Analysis Date = 05/12/13 Pct Recovery = 79% Analysis Date = 05/12/13 Pct Recovery = 79% Analysis Date = 05/02/13 Pct Recovery = 79% Analysis Date = 05/02/13 Pct Recovery = 79% Analysis Date = 04/23/13 Pct Recovery = 79% Analysis Date = 04/23/13 Pct Recovery = 79% Analysis Date = 04/13/13 Pct Recovery = 79% Analysis Date = 04/13/13 Pct Recovery = 79% Analysis Date = 04/03/13 Pct Recovery = 78% Analysis Date = 04/03/13 Pct Recovery = 78% Analysis Date = 03/24/13 Pct Recovery = 78% Analysis Date = 03/24/13 Pct Recovery = 78% Analysis Date = 03/14/13 Pct Recovery = 78% Analysis Date = 03/14/13 Pct Recovery = 78% Analysis Date = 03/05/13 Pct Recovery = 78% Analysis Date = 03/05/13 Pct Recovery = 78% Analysis Date = 02/23/13 Pct Recovery = 77% Analysis Date = 02/23/13 Pct Recovery = 77% Analysis Date = 02/13/13 Pct Recovery = 77% Analysis Date = 02/13/13 Pct Recovery = 77% Analysis Date = 02/03/13 Pct Recovery = 77% Analysis Date = 02/03/13 Pct Recovery = 77% Analysis Date = 01/24/13 Pct Recovery = 77% Analysis Date = 01/24/13 Pct Recovery = 77% Analysis Date = 01/15/13 Pct Recovery = 76% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
IPRODIONE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 69 93% 18% 93% 17%
Total 69 93% 18% 93% 17%

Sample Statistics
IPRODIONE

Characteristic N % % Basis
Plotted 69 100% Spiked
Estimated Values 69 100% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 69 .  
False Negatives 0 0% 0 out of 69
Not Spiked 57 .  
False Positives 0 0% 0 out of 57

OBSP Determination:
ISOFENPHOS
METHOD: 2033 , TESTIDCODE: 61594GCM39

Laboratory ID = 20130250061 Lab Value = 0.390 Expected Conc. = 0.5 Report level label = 0.014 Pct Recovery = 78% Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl SpecificMix = A088380 Laboratory ID = 20140230082 Lab Value = 0.168 Expected Conc. = 0.25 Report level label = 0.014 Pct Recovery = 67% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl SpecificMix = A093651 Laboratory ID = 20132420001 Lab Value = 0.193 Expected Conc. = 0.25 Report level label = 0.014 Pct Recovery = 77% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl SpecificMix = A093651 Laboratory ID = 20130810108 Lab Value = 0.253 Expected Conc. = 0.2495 Report level label = 0.014 Pct Recovery = 101% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl SpecificMix = T1120530013 Laboratory ID = 20123560092 Lab Value = 0.231 Expected Conc. = 0.2495 Report level label = 0.014 Pct Recovery = 93% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = T1120530013 Laboratory ID = 20132140002 Lab Value = 0.090 Expected Conc. = 0.1002 Report level label = 0.014 Pct Recovery = 90% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl SpecificMix = LB99392 Laboratory ID = 20131370001 Lab Value = 0.100 Expected Conc. = 0.1002 Report level label = 0.014 Pct Recovery = 100% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl SpecificMix = LB99392 Laboratory ID = 20140860102 Lab Value = 0.063 Expected Conc. = 0.1 Report level label = 0.014 Pct Recovery = 63% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl SpecificMix = A093651 Laboratory ID = 20133400002 Lab Value = 0.087 Expected Conc. = 0.1 Report level label = 0.014 Pct Recovery = 87% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = A093651 Laboratory ID = 20132910008 Lab Value = 0.081 Expected Conc. = 0.1 Report level label = 0.014 Pct Recovery = 81% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = A093651 Laboratory ID = 20131920149 Lab Value = 0.086 Expected Conc. = 0.1 Report level label = 0.014 Pct Recovery = 86% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl SpecificMix = A093651 Laboratory ID = 20131230084 Lab Value = 0.088 Expected Conc. = 0.1 Report level label = 0.014 Pct Recovery = 88% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl SpecificMix = A088380 Laboratory ID = 20130650005 Lab Value = 0.063 Expected Conc. = 0.1 Report level label = 0.014 Pct Recovery = 63% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl SpecificMix = A088380 Laboratory ID = 20130390105 Lab Value = 0.069 Expected Conc. = 0.0998 Report level label = 0.014 Pct Recovery = 69% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl SpecificMix = T1120530013 Laboratory ID = 20172510330 Lab Value = 0.085 Expected Conc. = 0.093 Report level label = 0.014 Pct Recovery = 92% Analysis Date = 12/29/17 SpikeMix = ChemService 6537100: 100 µl & Abs 071817Pest: 100 µl SpecificMix = 6537100 Laboratory ID = 20162860079 Lab Value = 0.096 Expected Conc. = 0.09 Report level label = 0.014 Pct Recovery = 106% Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl SpecificMix = 5054800 Laboratory ID = 20161880109 Lab Value = 0.107 Expected Conc. = 0.09 Report level label = 0.014 Pct Recovery = 119% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl SpecificMix = 5054800 Laboratory ID = 20163370001 Lab Value = 0.077 Expected Conc. = 0.0875 Report level label = 0.014 Pct Recovery = 88% Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl SpecificMix = LC20138V Laboratory ID = 20152460215 Lab Value = 0.029 Expected Conc. = 0.084 Report level label = 0.014 Pct Recovery = 35% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl SpecificMix = EN150514012 Laboratory ID = 20171380001 Lab Value = 0.054 Expected Conc. = 0.072 Report level label = 0.014 Pct Recovery = 75% Analysis Date = 06/07/17 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 5054800 Laboratory ID = 20170960001 Lab Value = 0.061 Expected Conc. = 0.072 Report level label = 0.014 Pct Recovery = 84% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl SpecificMix = 5054800 Laboratory ID = 20161740258 Lab Value = 0.053 Expected Conc. = 0.072 Report level label = 0.014 Pct Recovery = 74% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 5054800 Laboratory ID = 20171720140 Lab Value = 0.073 Expected Conc. = 0.07 Report level label = 0.014 Pct Recovery = 104% Analysis Date = 08/31/17 SpikeMix = Supelco LC20138V: 80 µl & Phenova B20160331: 80 µl SpecificMix = LC20138V Laboratory ID = 20170740063 Lab Value = 0.069 Expected Conc. = 0.07 Report level label = 0.014 Pct Recovery = 98% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl SpecificMix = LC20138V Laboratory ID = 20161470001 Lab Value = 0.075 Expected Conc. = 0.07 Report level label = 0.014 Pct Recovery = 107% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl SpecificMix = LC20138V Laboratory ID = 20150430092 Lab Value = 0.047 Expected Conc. = 0.0559 Report level label = 0.014 Pct Recovery = 85% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl SpecificMix = E1140407002 Laboratory ID = 20143110108 Lab Value = 0.045 Expected Conc. = 0.0559 Report level label = 0.014 Pct Recovery = 80% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl SpecificMix = E1140407002 Laboratory ID = 20142720002 Lab Value = 0.045 Expected Conc. = 0.0559 Report level label = 0.014 Pct Recovery = 80% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl SpecificMix = E1140407002 Laboratory ID = 20141770149 Lab Value = 0.045 Expected Conc. = 0.0559 Report level label = 0.014 Pct Recovery = 80% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl SpecificMix = E1140407002 Laboratory ID = 20143240095 Lab Value = 0.058 Expected Conc. = 0.0558 Report level label = 0.014 Pct Recovery = 103% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl SpecificMix = 032714 Laboratory ID = 20142270001 Lab Value = 0.043 Expected Conc. = 0.0558 Report level label = 0.014 Pct Recovery = 77% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl SpecificMix = 032714 Laboratory ID = 20141220025 Lab Value = 0.063 Expected Conc. = 0.0558 Report level label = 0.014 Pct Recovery = 113% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl SpecificMix = 032714 Laboratory ID = 20172370001 Lab Value = 0.042 Expected Conc. = 0.0465 Report level label = 0.014 Pct Recovery = 91% Analysis Date = 11/18/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6537100: 50 µl SpecificMix = 6537100 Laboratory ID = 20172230001 Lab Value = 0.050 Expected Conc. = 0.0465 Report level label = 0.014 Pct Recovery = 108% Analysis Date = 10/19/17 SpikeMix = ChemService 6472100: 50 µl & Abs 071717Pest: 50 µl SpecificMix = 071717Pest Laboratory ID = 20160630046 Lab Value = 0.031 Expected Conc. = 0.042 Report level label = 0.014 Pct Recovery = 74% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = EN150514012 Laboratory ID = 20153440001 Lab Value = 0.037 Expected Conc. = 0.042 Report level label = 0.014 Pct Recovery = 87% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = EN150514012 Laboratory ID = 20151900132 Lab Value = 0.004 Expected Conc. = 0.042 Report level label = 0.014 Pct Recovery = 9% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl SpecificMix = 041415 Laboratory ID = 20151270112 Lab Value = 0.042 Expected Conc. = 0.042 Report level label = 0.014 Pct Recovery = 100% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl SpecificMix = 041415 Laboratory ID = 20140510043 Lab Value = 0.028 Expected Conc. = 0.0401 Report level label = 0.014 Pct Recovery = 70% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl SpecificMix = LB99392 Laboratory ID = 20133470008 Lab Value = 0.036 Expected Conc. = 0.0401 Report level label = 0.014 Pct Recovery = 90% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl SpecificMix = LB99392 Laboratory ID = 20133190012 Lab Value = 0.040 Expected Conc. = 0.0401 Report level label = 0.014 Pct Recovery = 100% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = LB99392 Laboratory ID = 20133050050 Lab Value = 0.048 Expected Conc. = 0.0401 Report level label = 0.014 Pct Recovery = 119% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl SpecificMix = LB99392 Laboratory ID = 20172020035 Lab Value = 0.045 Expected Conc. = 0.0372 Report level label = 0.014 Pct Recovery = 121% Analysis Date = 11/07/17 SpikeMix = Abs 071717Pest: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 071717Pest Laboratory ID = 20171940002 Lab Value = 0.034 Expected Conc. = 0.036 Report level label = 0.014 Pct Recovery = 95% Analysis Date = 11/10/17 SpikeMix = ChemService 5054800: 40 µl & NSI 041816: 40 µl SpecificMix = 5054800 Laboratory ID = 20170460061 Lab Value = 0.032 Expected Conc. = 0.036 Report level label = 0.014 Pct Recovery = 89% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl SpecificMix = 5054800 Laboratory ID = 20163560019 Lab Value = 0.033 Expected Conc. = 0.036 Report level label = 0.014 Pct Recovery = 91% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl SpecificMix = 5054800 Laboratory ID = 20162150213 Lab Value = 0.036 Expected Conc. = 0.036 Report level label = 0.014 Pct Recovery = 100% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl SpecificMix = 5054800 Laboratory ID = 20171510080 Lab Value = 0.034 Expected Conc. = 0.035 Report level label = 0.014 Pct Recovery = 97% Analysis Date = 06/09/17 SpikeMix = Supelco LC20138V: 40 µl & Crescent 03FF076: 40 µl SpecificMix = LC20138V Laboratory ID = 20162520001 Lab Value = 0.045 Expected Conc. = 0.035 Report level label = 0.014 Pct Recovery = 128% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl SpecificMix = LC20138V Laboratory ID = 20162660005 Lab Value = 0.036 Expected Conc. = 0.035 Report level label = 0.014 Pct Recovery = 103% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl SpecificMix = LC20138V Laboratory ID = 20162020124 Lab Value = 0.033 Expected Conc. = 0.035 Report level label = 0.014 Pct Recovery = 94% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl SpecificMix = LC20138V Laboratory ID = 20142470041 Lab Value = 0.028 Expected Conc. = 0.028 Report level label = 0.014 Pct Recovery = 101% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141910243 Lab Value = 0.021 Expected Conc. = 0.028 Report level label = 0.014 Pct Recovery = 75% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141640076 Lab Value = 0.033 Expected Conc. = 0.028 Report level label = 0.014 Pct Recovery = 119% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141360094 Lab Value = 0.020 Expected Conc. = 0.028 Report level label = 0.014 Pct Recovery = 71% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = E1140407002 Laboratory ID = 20173120093 Lab Value = 0.033 Expected Conc. = 0.0279 Report level label = 0.014 Pct Recovery = 118% Analysis Date = 03/10/18 SpikeMix = ChemService 6472100: 30 µl & ChemService 6537100: 30 µl SpecificMix = 6537100 Laboratory ID = 20172780018 Lab Value = 0.025 Expected Conc. = 0.0279 Report level label = 0.014 Pct Recovery = 91% Analysis Date = 02/08/18 SpikeMix = ChemService 6537100: 30 µl & Abs 071817Pest: 30 µl SpecificMix = 6537100 Laboratory ID = 20150150115 Lab Value = 0.030 Expected Conc. = 0.0279 Report level label = 0.014 Pct Recovery = 106% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl SpecificMix = 032714 Laboratory ID = 20142820151 Lab Value = 0.029 Expected Conc. = 0.0279 Report level label = 0.014 Pct Recovery = 105% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl SpecificMix = 032714 Laboratory ID = 20141490205 Lab Value = 0.035 Expected Conc. = 0.0279 Report level label = 0.014 Pct Recovery = 125% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = 032714 Laboratory ID = 20141080004 Lab Value = 0.026 Expected Conc. = 0.0279 Report level label = 0.014 Pct Recovery = 93% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl SpecificMix = 032714 Laboratory ID = 20161050143 Lab Value = 0.020 Expected Conc. = 0.021 Report level label = 0.014 Pct Recovery = 93% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 041415 Laboratory ID = 20160560044 Lab Value = 0.018 Expected Conc. = 0.021 Report level label = 0.014 Pct Recovery = 87% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl SpecificMix = 041415 Laboratory ID = 20160210080 Lab Value = 0.015 Expected Conc. = 0.021 Report level label = 0.014 Pct Recovery = 70% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 041415 Laboratory ID = 20160070059 Lab Value = 0.021 Expected Conc. = 0.021 Report level label = 0.014 Pct Recovery = 99% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = EN150514012 Laboratory ID = 20153160001 Lab Value = 0.017 Expected Conc. = 0.021 Report level label = 0.014 Pct Recovery = 83% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = EN150514012 Laboratory ID = 20152950078 Lab Value = 0.012 Expected Conc. = 0.021 Report level label = 0.014 Pct Recovery = 57% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 041415 Laboratory ID = 20152040177 Lab Value = 0.011 Expected Conc. = 0.021 Report level label = 0.014 Pct Recovery = 53% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl SpecificMix = 041415 Laboratory ID = 20151760208 Lab Value = 0.004 Expected Conc. = 0.021 Report level label = 0.014 Pct Recovery = 18% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl SpecificMix = EN150514012 Laboratory ID = 20151480170 Lab Value = 0.020 Expected Conc. = 0.021 Report level label = 0.014 Pct Recovery = 95% Analysis Date = 06/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150514012 Laboratory ID = 20151210037 Lab Value = 0.023 Expected Conc. = 0.021 Report level label = 0.014 Pct Recovery = 109% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 041415 Analysis Date = 03/10/18 Pct Recovery = 107% Analysis Date = 02/28/18 Pct Recovery = 107% Analysis Date = 02/28/18 Pct Recovery = 107% Analysis Date = 02/19/18 Pct Recovery = 106% Analysis Date = 02/19/18 Pct Recovery = 106% Analysis Date = 02/09/18 Pct Recovery = 106% Analysis Date = 02/09/18 Pct Recovery = 106% Analysis Date = 01/31/18 Pct Recovery = 106% Analysis Date = 01/31/18 Pct Recovery = 106% Analysis Date = 01/22/18 Pct Recovery = 105% Analysis Date = 01/22/18 Pct Recovery = 105% Analysis Date = 01/12/18 Pct Recovery = 105% Analysis Date = 01/12/18 Pct Recovery = 105% Analysis Date = 01/03/18 Pct Recovery = 105% Analysis Date = 01/03/18 Pct Recovery = 105% Analysis Date = 12/24/17 Pct Recovery = 104% Analysis Date = 12/24/17 Pct Recovery = 104% Analysis Date = 12/15/17 Pct Recovery = 104% Analysis Date = 12/15/17 Pct Recovery = 104% Analysis Date = 12/06/17 Pct Recovery = 104% Analysis Date = 12/06/17 Pct Recovery = 104% Analysis Date = 11/26/17 Pct Recovery = 104% Analysis Date = 11/26/17 Pct Recovery = 104% Analysis Date = 11/17/17 Pct Recovery = 103% Analysis Date = 11/17/17 Pct Recovery = 103% Analysis Date = 11/07/17 Pct Recovery = 103% Analysis Date = 11/07/17 Pct Recovery = 103% Analysis Date = 10/29/17 Pct Recovery = 103% Analysis Date = 10/29/17 Pct Recovery = 103% Analysis Date = 10/20/17 Pct Recovery = 102% Analysis Date = 10/20/17 Pct Recovery = 102% Analysis Date = 10/10/17 Pct Recovery = 102% Analysis Date = 10/10/17 Pct Recovery = 102% Analysis Date = 10/01/17 Pct Recovery = 102% Analysis Date = 10/01/17 Pct Recovery = 102% Analysis Date = 09/21/17 Pct Recovery = 102% Analysis Date = 09/21/17 Pct Recovery = 102% Analysis Date = 09/12/17 Pct Recovery = 101% Analysis Date = 09/12/17 Pct Recovery = 101% Analysis Date = 09/03/17 Pct Recovery = 101% Analysis Date = 09/03/17 Pct Recovery = 101% Analysis Date = 08/24/17 Pct Recovery = 101% Analysis Date = 08/24/17 Pct Recovery = 101% Analysis Date = 08/15/17 Pct Recovery = 100% Analysis Date = 08/15/17 Pct Recovery = 100% Analysis Date = 08/05/17 Pct Recovery = 100% Analysis Date = 08/05/17 Pct Recovery = 100% Analysis Date = 07/27/17 Pct Recovery = 100% Analysis Date = 07/27/17 Pct Recovery = 100% Analysis Date = 07/18/17 Pct Recovery = 100% Analysis Date = 07/18/17 Pct Recovery = 100% Analysis Date = 07/08/17 Pct Recovery = 99% Analysis Date = 07/08/17 Pct Recovery = 99% Analysis Date = 06/29/17 Pct Recovery = 99% Analysis Date = 06/29/17 Pct Recovery = 99% Analysis Date = 06/19/17 Pct Recovery = 99% Analysis Date = 06/19/17 Pct Recovery = 99% Analysis Date = 06/10/17 Pct Recovery = 98% Analysis Date = 06/10/17 Pct Recovery = 98% Analysis Date = 06/01/17 Pct Recovery = 98% Analysis Date = 06/01/17 Pct Recovery = 98% Analysis Date = 05/22/17 Pct Recovery = 98% Analysis Date = 05/22/17 Pct Recovery = 98% Analysis Date = 05/13/17 Pct Recovery = 97% Analysis Date = 05/13/17 Pct Recovery = 97% Analysis Date = 05/03/17 Pct Recovery = 97% Analysis Date = 05/03/17 Pct Recovery = 97% Analysis Date = 04/24/17 Pct Recovery = 97% Analysis Date = 04/24/17 Pct Recovery = 97% Analysis Date = 04/15/17 Pct Recovery = 96% Analysis Date = 04/15/17 Pct Recovery = 96% Analysis Date = 04/05/17 Pct Recovery = 96% Analysis Date = 04/05/17 Pct Recovery = 96% Analysis Date = 03/27/17 Pct Recovery = 96% Analysis Date = 03/27/17 Pct Recovery = 96% Analysis Date = 03/17/17 Pct Recovery = 95% Analysis Date = 03/17/17 Pct Recovery = 95% Analysis Date = 03/08/17 Pct Recovery = 95% Analysis Date = 03/08/17 Pct Recovery = 95% Analysis Date = 02/27/17 Pct Recovery = 95% Analysis Date = 02/27/17 Pct Recovery = 95% Analysis Date = 02/17/17 Pct Recovery = 94% Analysis Date = 02/17/17 Pct Recovery = 94% Analysis Date = 02/08/17 Pct Recovery = 94% Analysis Date = 02/08/17 Pct Recovery = 94% Analysis Date = 01/29/17 Pct Recovery = 94% Analysis Date = 01/29/17 Pct Recovery = 94% Analysis Date = 01/20/17 Pct Recovery = 93% Analysis Date = 01/20/17 Pct Recovery = 93% Analysis Date = 01/11/17 Pct Recovery = 93% Analysis Date = 01/11/17 Pct Recovery = 93% Analysis Date = 01/01/17 Pct Recovery = 93% Analysis Date = 01/01/17 Pct Recovery = 93% Analysis Date = 12/23/16 Pct Recovery = 92% Analysis Date = 12/23/16 Pct Recovery = 92% Analysis Date = 12/13/16 Pct Recovery = 92% Analysis Date = 12/13/16 Pct Recovery = 92% Analysis Date = 12/04/16 Pct Recovery = 91% Analysis Date = 12/04/16 Pct Recovery = 91% Analysis Date = 11/25/16 Pct Recovery = 91% Analysis Date = 11/25/16 Pct Recovery = 91% Analysis Date = 11/15/16 Pct Recovery = 91% Analysis Date = 11/15/16 Pct Recovery = 91% Analysis Date = 11/06/16 Pct Recovery = 90% Analysis Date = 11/06/16 Pct Recovery = 90% Analysis Date = 10/27/16 Pct Recovery = 90% Analysis Date = 10/27/16 Pct Recovery = 90% Analysis Date = 10/18/16 Pct Recovery = 90% Analysis Date = 10/18/16 Pct Recovery = 90% Analysis Date = 10/09/16 Pct Recovery = 89% Analysis Date = 10/09/16 Pct Recovery = 89% Analysis Date = 09/29/16 Pct Recovery = 89% Analysis Date = 09/29/16 Pct Recovery = 89% Analysis Date = 09/20/16 Pct Recovery = 89% Analysis Date = 09/20/16 Pct Recovery = 89% Analysis Date = 09/10/16 Pct Recovery = 88% Analysis Date = 09/10/16 Pct Recovery = 88% Analysis Date = 09/01/16 Pct Recovery = 88% Analysis Date = 09/01/16 Pct Recovery = 88% Analysis Date = 08/23/16 Pct Recovery = 87% Analysis Date = 08/23/16 Pct Recovery = 87% Analysis Date = 08/13/16 Pct Recovery = 87% Analysis Date = 08/13/16 Pct Recovery = 87% Analysis Date = 08/04/16 Pct Recovery = 87% Analysis Date = 08/04/16 Pct Recovery = 87% Analysis Date = 07/25/16 Pct Recovery = 86% Analysis Date = 07/25/16 Pct Recovery = 86% Analysis Date = 07/16/16 Pct Recovery = 86% Analysis Date = 07/16/16 Pct Recovery = 86% Analysis Date = 07/07/16 Pct Recovery = 86% Analysis Date = 07/07/16 Pct Recovery = 86% Analysis Date = 06/27/16 Pct Recovery = 85% Analysis Date = 06/27/16 Pct Recovery = 85% Analysis Date = 06/18/16 Pct Recovery = 85% Analysis Date = 06/18/16 Pct Recovery = 85% Analysis Date = 06/08/16 Pct Recovery = 85% Analysis Date = 06/08/16 Pct Recovery = 85% Analysis Date = 05/30/16 Pct Recovery = 84% Analysis Date = 05/30/16 Pct Recovery = 84% Analysis Date = 05/21/16 Pct Recovery = 84% Analysis Date = 05/21/16 Pct Recovery = 84% Analysis Date = 05/11/16 Pct Recovery = 84% Analysis Date = 05/11/16 Pct Recovery = 84% Analysis Date = 05/02/16 Pct Recovery = 84% Analysis Date = 05/02/16 Pct Recovery = 84% Analysis Date = 04/22/16 Pct Recovery = 83% Analysis Date = 04/22/16 Pct Recovery = 83% Analysis Date = 04/13/16 Pct Recovery = 83% Analysis Date = 04/13/16 Pct Recovery = 83% Analysis Date = 04/04/16 Pct Recovery = 83% Analysis Date = 04/04/16 Pct Recovery = 83% Analysis Date = 03/25/16 Pct Recovery = 82% Analysis Date = 03/25/16 Pct Recovery = 82% Analysis Date = 03/16/16 Pct Recovery = 82% Analysis Date = 03/16/16 Pct Recovery = 82% Analysis Date = 03/06/16 Pct Recovery = 82% Analysis Date = 03/06/16 Pct Recovery = 82% Analysis Date = 02/26/16 Pct Recovery = 81% Analysis Date = 02/26/16 Pct Recovery = 81% Analysis Date = 02/17/16 Pct Recovery = 81% Analysis Date = 02/17/16 Pct Recovery = 81% Analysis Date = 02/07/16 Pct Recovery = 81% Analysis Date = 02/07/16 Pct Recovery = 81% Analysis Date = 01/29/16 Pct Recovery = 80% Analysis Date = 01/29/16 Pct Recovery = 80% Analysis Date = 01/19/16 Pct Recovery = 80% Analysis Date = 01/19/16 Pct Recovery = 80% Analysis Date = 01/10/16 Pct Recovery = 80% Analysis Date = 01/10/16 Pct Recovery = 80% Analysis Date = 01/01/16 Pct Recovery = 80% Analysis Date = 01/01/16 Pct Recovery = 80% Analysis Date = 12/22/15 Pct Recovery = 80% Analysis Date = 12/22/15 Pct Recovery = 80% Analysis Date = 12/13/15 Pct Recovery = 80% Analysis Date = 12/13/15 Pct Recovery = 80% Analysis Date = 12/03/15 Pct Recovery = 80% Analysis Date = 12/03/15 Pct Recovery = 80% Analysis Date = 11/24/15 Pct Recovery = 80% Analysis Date = 11/24/15 Pct Recovery = 80% Analysis Date = 11/15/15 Pct Recovery = 80% Analysis Date = 11/15/15 Pct Recovery = 80% Analysis Date = 11/05/15 Pct Recovery = 80% Analysis Date = 11/05/15 Pct Recovery = 80% Analysis Date = 10/27/15 Pct Recovery = 80% Analysis Date = 10/27/15 Pct Recovery = 80% Analysis Date = 10/17/15 Pct Recovery = 80% Analysis Date = 10/17/15 Pct Recovery = 80% Analysis Date = 10/08/15 Pct Recovery = 80% Analysis Date = 10/08/15 Pct Recovery = 80% Analysis Date = 09/29/15 Pct Recovery = 80% Analysis Date = 09/29/15 Pct Recovery = 80% Analysis Date = 09/19/15 Pct Recovery = 80% Analysis Date = 09/19/15 Pct Recovery = 80% Analysis Date = 09/10/15 Pct Recovery = 80% Analysis Date = 09/10/15 Pct Recovery = 80% Analysis Date = 08/31/15 Pct Recovery = 80% Analysis Date = 08/31/15 Pct Recovery = 80% Analysis Date = 08/22/15 Pct Recovery = 80% Analysis Date = 08/22/15 Pct Recovery = 80% Analysis Date = 08/13/15 Pct Recovery = 80% Analysis Date = 08/13/15 Pct Recovery = 80% Analysis Date = 08/03/15 Pct Recovery = 80% Analysis Date = 08/03/15 Pct Recovery = 80% Analysis Date = 07/25/15 Pct Recovery = 80% Analysis Date = 07/25/15 Pct Recovery = 80% Analysis Date = 07/15/15 Pct Recovery = 80% Analysis Date = 07/15/15 Pct Recovery = 80% Analysis Date = 07/06/15 Pct Recovery = 80% Analysis Date = 07/06/15 Pct Recovery = 80% Analysis Date = 06/27/15 Pct Recovery = 80% Analysis Date = 06/27/15 Pct Recovery = 80% Analysis Date = 06/17/15 Pct Recovery = 80% Analysis Date = 06/17/15 Pct Recovery = 80% Analysis Date = 06/08/15 Pct Recovery = 80% Analysis Date = 06/08/15 Pct Recovery = 80% Analysis Date = 05/29/15 Pct Recovery = 80% Analysis Date = 05/29/15 Pct Recovery = 80% Analysis Date = 05/20/15 Pct Recovery = 80% Analysis Date = 05/20/15 Pct Recovery = 80% Analysis Date = 05/11/15 Pct Recovery = 80% Analysis Date = 05/11/15 Pct Recovery = 80% Analysis Date = 05/01/15 Pct Recovery = 80% Analysis Date = 05/01/15 Pct Recovery = 80% Analysis Date = 04/22/15 Pct Recovery = 80% Analysis Date = 04/22/15 Pct Recovery = 80% Analysis Date = 04/12/15 Pct Recovery = 80% Analysis Date = 04/12/15 Pct Recovery = 80% Analysis Date = 04/03/15 Pct Recovery = 80% Analysis Date = 04/03/15 Pct Recovery = 80% Analysis Date = 03/25/15 Pct Recovery = 80% Analysis Date = 03/25/15 Pct Recovery = 80% Analysis Date = 03/15/15 Pct Recovery = 80% Analysis Date = 03/15/15 Pct Recovery = 80% Analysis Date = 03/06/15 Pct Recovery = 80% Analysis Date = 03/06/15 Pct Recovery = 80% Analysis Date = 02/24/15 Pct Recovery = 81% Analysis Date = 02/24/15 Pct Recovery = 81% Analysis Date = 02/15/15 Pct Recovery = 81% Analysis Date = 02/15/15 Pct Recovery = 81% Analysis Date = 02/06/15 Pct Recovery = 81% Analysis Date = 02/06/15 Pct Recovery = 81% Analysis Date = 01/27/15 Pct Recovery = 81% Analysis Date = 01/27/15 Pct Recovery = 81% Analysis Date = 01/18/15 Pct Recovery = 81% Analysis Date = 01/18/15 Pct Recovery = 81% Analysis Date = 01/08/15 Pct Recovery = 82% Analysis Date = 01/08/15 Pct Recovery = 82% Analysis Date = 12/30/14 Pct Recovery = 82% Analysis Date = 12/30/14 Pct Recovery = 82% Analysis Date = 12/21/14 Pct Recovery = 82% Analysis Date = 12/21/14 Pct Recovery = 82% Analysis Date = 12/11/14 Pct Recovery = 83% Analysis Date = 12/11/14 Pct Recovery = 83% Analysis Date = 12/02/14 Pct Recovery = 83% Analysis Date = 12/02/14 Pct Recovery = 83% Analysis Date = 11/22/14 Pct Recovery = 83% Analysis Date = 11/22/14 Pct Recovery = 83% Analysis Date = 11/13/14 Pct Recovery = 83% Analysis Date = 11/13/14 Pct Recovery = 83% Analysis Date = 11/04/14 Pct Recovery = 84% Analysis Date = 11/04/14 Pct Recovery = 84% Analysis Date = 10/25/14 Pct Recovery = 84% Analysis Date = 10/25/14 Pct Recovery = 84% Analysis Date = 10/16/14 Pct Recovery = 84% Analysis Date = 10/16/14 Pct Recovery = 84% Analysis Date = 10/06/14 Pct Recovery = 85% Analysis Date = 10/06/14 Pct Recovery = 85% Analysis Date = 09/27/14 Pct Recovery = 85% Analysis Date = 09/27/14 Pct Recovery = 85% Analysis Date = 09/18/14 Pct Recovery = 85% Analysis Date = 09/18/14 Pct Recovery = 85% Analysis Date = 09/08/14 Pct Recovery = 86% Analysis Date = 09/08/14 Pct Recovery = 86% Analysis Date = 08/30/14 Pct Recovery = 86% Analysis Date = 08/30/14 Pct Recovery = 86% Analysis Date = 08/20/14 Pct Recovery = 86% Analysis Date = 08/20/14 Pct Recovery = 86% Analysis Date = 08/11/14 Pct Recovery = 87% Analysis Date = 08/11/14 Pct Recovery = 87% Analysis Date = 08/02/14 Pct Recovery = 87% Analysis Date = 08/02/14 Pct Recovery = 87% Analysis Date = 07/23/14 Pct Recovery = 87% Analysis Date = 07/23/14 Pct Recovery = 87% Analysis Date = 07/14/14 Pct Recovery = 87% Analysis Date = 07/14/14 Pct Recovery = 87% Analysis Date = 07/04/14 Pct Recovery = 88% Analysis Date = 07/04/14 Pct Recovery = 88% Analysis Date = 06/25/14 Pct Recovery = 88% Analysis Date = 06/25/14 Pct Recovery = 88% Analysis Date = 06/16/14 Pct Recovery = 88% Analysis Date = 06/16/14 Pct Recovery = 88% Analysis Date = 06/06/14 Pct Recovery = 88% Analysis Date = 06/06/14 Pct Recovery = 88% Analysis Date = 05/28/14 Pct Recovery = 88% Analysis Date = 05/28/14 Pct Recovery = 88% Analysis Date = 05/18/14 Pct Recovery = 88% Analysis Date = 05/18/14 Pct Recovery = 88% Analysis Date = 05/09/14 Pct Recovery = 88% Analysis Date = 05/09/14 Pct Recovery = 88% Analysis Date = 04/30/14 Pct Recovery = 88% Analysis Date = 04/30/14 Pct Recovery = 88% Analysis Date = 04/20/14 Pct Recovery = 88% Analysis Date = 04/20/14 Pct Recovery = 88% Analysis Date = 04/11/14 Pct Recovery = 88% Analysis Date = 04/11/14 Pct Recovery = 88% Analysis Date = 04/01/14 Pct Recovery = 88% Analysis Date = 04/01/14 Pct Recovery = 88% Analysis Date = 03/23/14 Pct Recovery = 88% Analysis Date = 03/23/14 Pct Recovery = 88% Analysis Date = 03/14/14 Pct Recovery = 88% Analysis Date = 03/14/14 Pct Recovery = 88% Analysis Date = 03/04/14 Pct Recovery = 88% Analysis Date = 03/04/14 Pct Recovery = 88% Analysis Date = 02/23/14 Pct Recovery = 88% Analysis Date = 02/23/14 Pct Recovery = 88% Analysis Date = 02/13/14 Pct Recovery = 88% Analysis Date = 02/13/14 Pct Recovery = 88% Analysis Date = 02/04/14 Pct Recovery = 88% Analysis Date = 02/04/14 Pct Recovery = 88% Analysis Date = 01/26/14 Pct Recovery = 88% Analysis Date = 01/26/14 Pct Recovery = 88% Analysis Date = 01/16/14 Pct Recovery = 88% Analysis Date = 01/16/14 Pct Recovery = 88% Analysis Date = 01/07/14 Pct Recovery = 88% Analysis Date = 01/07/14 Pct Recovery = 88% Analysis Date = 12/28/13 Pct Recovery = 88% Analysis Date = 12/28/13 Pct Recovery = 88% Analysis Date = 12/19/13 Pct Recovery = 88% Analysis Date = 12/19/13 Pct Recovery = 88% Analysis Date = 12/10/13 Pct Recovery = 88% Analysis Date = 12/10/13 Pct Recovery = 88% Analysis Date = 11/30/13 Pct Recovery = 88% Analysis Date = 11/30/13 Pct Recovery = 88% Analysis Date = 11/21/13 Pct Recovery = 88% Analysis Date = 11/21/13 Pct Recovery = 88% Analysis Date = 11/11/13 Pct Recovery = 88% Analysis Date = 11/11/13 Pct Recovery = 88% Analysis Date = 11/02/13 Pct Recovery = 87% Analysis Date = 11/02/13 Pct Recovery = 87% Analysis Date = 10/24/13 Pct Recovery = 87% Analysis Date = 10/24/13 Pct Recovery = 87% Analysis Date = 10/14/13 Pct Recovery = 87% Analysis Date = 10/14/13 Pct Recovery = 87% Analysis Date = 10/05/13 Pct Recovery = 87% Analysis Date = 10/05/13 Pct Recovery = 87% Analysis Date = 09/25/13 Pct Recovery = 87% Analysis Date = 09/25/13 Pct Recovery = 87% Analysis Date = 09/16/13 Pct Recovery = 87% Analysis Date = 09/16/13 Pct Recovery = 87% Analysis Date = 09/07/13 Pct Recovery = 87% Analysis Date = 09/07/13 Pct Recovery = 87% Analysis Date = 08/28/13 Pct Recovery = 87% Analysis Date = 08/28/13 Pct Recovery = 87% Analysis Date = 08/19/13 Pct Recovery = 87% Analysis Date = 08/19/13 Pct Recovery = 87% Analysis Date = 08/09/13 Pct Recovery = 87% Analysis Date = 08/09/13 Pct Recovery = 87% Analysis Date = 07/31/13 Pct Recovery = 87% Analysis Date = 07/31/13 Pct Recovery = 87% Analysis Date = 07/22/13 Pct Recovery = 87% Analysis Date = 07/22/13 Pct Recovery = 87% Analysis Date = 07/12/13 Pct Recovery = 87% Analysis Date = 07/12/13 Pct Recovery = 87% Analysis Date = 07/03/13 Pct Recovery = 87% Analysis Date = 07/03/13 Pct Recovery = 87% Analysis Date = 06/23/13 Pct Recovery = 87% Analysis Date = 06/23/13 Pct Recovery = 87% Analysis Date = 06/14/13 Pct Recovery = 87% Analysis Date = 06/14/13 Pct Recovery = 87% Analysis Date = 06/05/13 Pct Recovery = 86% Analysis Date = 06/05/13 Pct Recovery = 86% Analysis Date = 05/26/13 Pct Recovery = 86% Analysis Date = 05/26/13 Pct Recovery = 86% Analysis Date = 05/17/13 Pct Recovery = 86% Analysis Date = 05/17/13 Pct Recovery = 86% Analysis Date = 05/07/13 Pct Recovery = 86% Analysis Date = 05/07/13 Pct Recovery = 86% Analysis Date = 04/28/13 Pct Recovery = 86% Analysis Date = 04/28/13 Pct Recovery = 86% Analysis Date = 04/19/13 Pct Recovery = 86% Analysis Date = 04/19/13 Pct Recovery = 86% Analysis Date = 04/09/13 Pct Recovery = 86% Analysis Date = 04/09/13 Pct Recovery = 86% Analysis Date = 03/31/13 Pct Recovery = 86% Analysis Date = 03/31/13 Pct Recovery = 86% Analysis Date = 03/21/13 Pct Recovery = 86% Analysis Date = 03/21/13 Pct Recovery = 86% Analysis Date = 03/12/13 Pct Recovery = 86% Analysis Date = 03/12/13 Pct Recovery = 86% Analysis Date = 03/03/13 Pct Recovery = 86% Analysis Date = 03/03/13 Pct Recovery = 86% Analysis Date = 02/21/13 Pct Recovery = 86% Analysis Date = 02/21/13 Pct Recovery = 86% Analysis Date = 02/12/13 Pct Recovery = 85% Analysis Date = 02/12/13 Pct Recovery = 85% Analysis Date = 02/02/13 Pct Recovery = 85% Analysis Date = 02/02/13 Pct Recovery = 85% Analysis Date = 01/24/13 Pct Recovery = 85% Analysis Date = 01/24/13 Pct Recovery = 85% Analysis Date = 01/15/13 Pct Recovery = 85% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
ISOFENPHOS

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 71 88% 22% 91% 18%
Total 71 88% 22% 91% 18%

Sample Statistics
ISOFENPHOS

Characteristic N % % Basis
Plotted 71 99% Spiked
Estimated Values 1 1% Spiked
Deleted Values 1 1% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 73 .  
False Negatives 1 1% 1 out of 72
Not Spiked 45 .  
False Positives 0 0% 0 out of 45

OBSP Determination:
MALAOXON
METHOD: 2033 , TESTIDCODE: 61652GCM39

Laboratory ID = 20140100085 Lab Value = 0.291 Expected Conc. = 0.241 Report level label = 0.022 Pct Recovery = 121% Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl SpecificMix = 042413 Laboratory ID = 20130250061 Lab Value = 0.109 Expected Conc. = 0.15 Report level label = 0.022 Pct Recovery = 73% Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl SpecificMix = 05BB029 Laboratory ID = 20172510330 Lab Value = 0.130 Expected Conc. = 0.147 Report level label = 0.022 Pct Recovery = 88% Analysis Date = 12/29/17 SpikeMix = ChemService 6537100: 100 µl & Abs 071817Pest: 100 µl SpecificMix = 071817Pest Laboratory ID = 20162860079 Lab Value = 0.120 Expected Conc. = 0.138 Report level label = 0.022 Pct Recovery = 87% Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl SpecificMix = 060916 Laboratory ID = 20163150006 Lab Value = 0.144 Expected Conc. = 0.138 Report level label = 0.022 Pct Recovery = 104% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl SpecificMix = 060916 Laboratory ID = 20152610011 Lab Value = 0.092 Expected Conc. = 0.132 Report level label = 0.022 Pct Recovery = 70% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl SpecificMix = 0406-15-01 Laboratory ID = 20152460215 Lab Value = 0.141 Expected Conc. = 0.132 Report level label = 0.022 Pct Recovery = 107% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl SpecificMix = 0406-15-01 Laboratory ID = 20132690010 Lab Value = 0.142 Expected Conc. = 0.1205 Report level label = 0.022 Pct Recovery = 118% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl SpecificMix = 042413 Laboratory ID = 20132560001 Lab Value = 0.107 Expected Conc. = 0.1205 Report level label = 0.022 Pct Recovery = 89% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl SpecificMix = 042413 Laboratory ID = 20132140002 Lab Value = 0.079 Expected Conc. = 0.12 Report level label = 0.022 Pct Recovery = 66% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl SpecificMix = 04CC101 Laboratory ID = 20171380001 Lab Value = 0.061 Expected Conc. = 0.1112 Report level label = 0.022 Pct Recovery = 55% Analysis Date = 06/07/17 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 041816 Laboratory ID = 20170740063 Lab Value = 0.049 Expected Conc. = 0.1112 Report level label = 0.022 Pct Recovery = 44% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl SpecificMix = 041816 Laboratory ID = 20161740258 Lab Value = 0.058 Expected Conc. = 0.1112 Report level label = 0.022 Pct Recovery = 52% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 041816 Laboratory ID = 20171660002 Lab Value = 0.138 Expected Conc. = 0.1104 Report level label = 0.022 Pct Recovery = 125% Analysis Date = 08/23/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = 060916 Laboratory ID = 20170190026 Lab Value = 0.110 Expected Conc. = 0.1104 Report level label = 0.022 Pct Recovery = 100% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = 060916 Laboratory ID = 20150430092 Lab Value = 0.071 Expected Conc. = 0.09 Report level label = 0.022 Pct Recovery = 79% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl SpecificMix = E1140407002 Laboratory ID = 20143110108 Lab Value = 0.071 Expected Conc. = 0.09 Report level label = 0.022 Pct Recovery = 79% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl SpecificMix = E1140407002 Laboratory ID = 20142720002 Lab Value = 0.072 Expected Conc. = 0.09 Report level label = 0.022 Pct Recovery = 80% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl SpecificMix = E1140407002 Laboratory ID = 20141770149 Lab Value = 0.077 Expected Conc. = 0.09 Report level label = 0.022 Pct Recovery = 86% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl SpecificMix = E1140407002 Laboratory ID = 20143240095 Lab Value = 0.109 Expected Conc. = 0.0882 Report level label = 0.022 Pct Recovery = 124% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl SpecificMix = 032714 Laboratory ID = 20142270001 Lab Value = 0.100 Expected Conc. = 0.0882 Report level label = 0.022 Pct Recovery = 113% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl SpecificMix = 032714 Laboratory ID = 20141220025 Lab Value = 0.096 Expected Conc. = 0.0882 Report level label = 0.022 Pct Recovery = 109% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl SpecificMix = 032714 Laboratory ID = 20130940097 Lab Value = 0.077 Expected Conc. = 0.076 Report level label = 0.022 Pct Recovery = 101% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = 052412 Laboratory ID = 20130100066 Lab Value = 0.089 Expected Conc. = 0.076 Report level label = 0.022 Pct Recovery = 117% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl SpecificMix = 052412 Laboratory ID = 20140230082 Lab Value = 0.074 Expected Conc. = 0.0755 Report level label = 0.022 Pct Recovery = 98% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl SpecificMix = 012513 Laboratory ID = 20132420001 Lab Value = 0.076 Expected Conc. = 0.0755 Report level label = 0.022 Pct Recovery = 101% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl SpecificMix = 012513 Laboratory ID = 20172560101 Lab Value = 0.067 Expected Conc. = 0.075 Report level label = 0.022 Pct Recovery = 89% Analysis Date = 12/22/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6567600: 50 µl SpecificMix = 6567600 Laboratory ID = 20161260151 Lab Value = 0.049 Expected Conc. = 0.068 Report level label = 0.022 Pct Recovery = 72% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = 3851600 Laboratory ID = 20151550293 Lab Value = 0.062 Expected Conc. = 0.068 Report level label = 0.022 Pct Recovery = 91% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl SpecificMix = 3851600 Laboratory ID = 20151270112 Lab Value = 0.064 Expected Conc. = 0.068 Report level label = 0.022 Pct Recovery = 94% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl SpecificMix = 3851600 Laboratory ID = 20160770090 Lab Value = 0.053 Expected Conc. = 0.066 Report level label = 0.022 Pct Recovery = 80% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20160630046 Lab Value = 0.059 Expected Conc. = 0.066 Report level label = 0.022 Pct Recovery = 89% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20153510109 Lab Value = 0.054 Expected Conc. = 0.066 Report level label = 0.022 Pct Recovery = 82% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20153440001 Lab Value = 0.063 Expected Conc. = 0.066 Report level label = 0.022 Pct Recovery = 95% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20171940002 Lab Value = 0.054 Expected Conc. = 0.0556 Report level label = 0.022 Pct Recovery = 97% Analysis Date = 11/10/17 SpikeMix = ChemService 5054800: 40 µl & NSI 041816: 40 µl SpecificMix = 041816 Laboratory ID = 20162020124 Lab Value = 0.037 Expected Conc. = 0.0556 Report level label = 0.022 Pct Recovery = 67% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl SpecificMix = 041816 Laboratory ID = 20161600087 Lab Value = 0.058 Expected Conc. = 0.0556 Report level label = 0.022 Pct Recovery = 104% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 041816 Laboratory ID = 20161340228 Lab Value = 0.050 Expected Conc. = 0.0556 Report level label = 0.022 Pct Recovery = 90% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl SpecificMix = 041816 Laboratory ID = 20161190075 Lab Value = 0.045 Expected Conc. = 0.0556 Report level label = 0.022 Pct Recovery = 81% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 041816 Laboratory ID = 20171160110 Lab Value = 0.051 Expected Conc. = 0.0552 Report level label = 0.022 Pct Recovery = 92% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = 060916 Laboratory ID = 20162520001 Lab Value = 0.066 Expected Conc. = 0.0552 Report level label = 0.022 Pct Recovery = 120% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl SpecificMix = 060916 Laboratory ID = 20163560019 Lab Value = 0.050 Expected Conc. = 0.0552 Report level label = 0.022 Pct Recovery = 91% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl SpecificMix = 060916 Laboratory ID = 20162380004 Lab Value = 0.069 Expected Conc. = 0.0552 Report level label = 0.022 Pct Recovery = 125% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = 060916 Laboratory ID = 20133580036 Lab Value = 0.059 Expected Conc. = 0.0482 Report level label = 0.022 Pct Recovery = 122% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 042413 Laboratory ID = 20133190012 Lab Value = 0.077 Expected Conc. = 0.0482 Report level label = 0.022 Pct Recovery = 160% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 042413 Laboratory ID = 20131650073 Lab Value = 0.068 Expected Conc. = 0.0482 Report level label = 0.022 Pct Recovery = 141% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl SpecificMix = 042413 Laboratory ID = 20140730138 Lab Value = 0.036 Expected Conc. = 0.048 Report level label = 0.022 Pct Recovery = 75% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 04CC101 Laboratory ID = 20140510043 Lab Value = 0.033 Expected Conc. = 0.048 Report level label = 0.022 Pct Recovery = 69% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 04CC101 Laboratory ID = 20133310030 Lab Value = 0.056 Expected Conc. = 0.048 Report level label = 0.022 Pct Recovery = 117% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl SpecificMix = 04CC101 Laboratory ID = 20132280016 Lab Value = 0.053 Expected Conc. = 0.048 Report level label = 0.022 Pct Recovery = 110% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl SpecificMix = 04CC101 Laboratory ID = 20131510026 Lab Value = 0.048 Expected Conc. = 0.048 Report level label = 0.022 Pct Recovery = 100% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl SpecificMix = 04CC101 Laboratory ID = 20142470041 Lab Value = 0.058 Expected Conc. = 0.045 Report level label = 0.022 Pct Recovery = 129% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141910243 Lab Value = 0.035 Expected Conc. = 0.045 Report level label = 0.022 Pct Recovery = 78% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141640076 Lab Value = 0.042 Expected Conc. = 0.045 Report level label = 0.022 Pct Recovery = 93% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141360094 Lab Value = 0.039 Expected Conc. = 0.045 Report level label = 0.022 Pct Recovery = 87% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = E1140407002 Laboratory ID = 20172780018 Lab Value = 0.036 Expected Conc. = 0.0441 Report level label = 0.022 Pct Recovery = 82% Analysis Date = 02/08/18 SpikeMix = ChemService 6537100: 30 µl & Abs 071817Pest: 30 µl SpecificMix = 071817Pest Laboratory ID = 20150150115 Lab Value = 0.046 Expected Conc. = 0.0441 Report level label = 0.022 Pct Recovery = 104% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl SpecificMix = 032714 Laboratory ID = 20142820151 Lab Value = 0.052 Expected Conc. = 0.0441 Report level label = 0.022 Pct Recovery = 118% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl SpecificMix = 032714 Laboratory ID = 20141490205 Lab Value = 0.060 Expected Conc. = 0.0441 Report level label = 0.022 Pct Recovery = 136% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = 032714 Laboratory ID = 20141080004 Lab Value = 0.046 Expected Conc. = 0.0441 Report level label = 0.022 Pct Recovery = 104% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl SpecificMix = 032714 Laboratory ID = 20160430111 Lab Value = 0.030 Expected Conc. = 0.034 Report level label = 0.022 Pct Recovery = 88% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 3851600 Laboratory ID = 20160210080 Lab Value = 0.023 Expected Conc. = 0.034 Report level label = 0.022 Pct Recovery = 68% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 3851600 Laboratory ID = 20152950078 Lab Value = 0.021 Expected Conc. = 0.034 Report level label = 0.022 Pct Recovery = 62% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 3851600 Laboratory ID = 20153030068 Lab Value = 0.025 Expected Conc. = 0.034 Report level label = 0.022 Pct Recovery = 74% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = 3851600 Laboratory ID = 20151760208 Lab Value = 0.047 Expected Conc. = 0.034 Report level label = 0.022 Pct Recovery = 138% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl SpecificMix = 3851600 Laboratory ID = 20152190003 Lab Value = 0.037 Expected Conc. = 0.033 Report level label = 0.022 Pct Recovery = 112% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = 0406-15-01 Laboratory ID = 20152040177 Lab Value = 0.041 Expected Conc. = 0.033 Report level label = 0.022 Pct Recovery = 124% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl SpecificMix = 0406-15-01 Laboratory ID = 20133400002 Lab Value = 0.038 Expected Conc. = 0.0304 Report level label = 0.022 Pct Recovery = 125% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = 052412 Laboratory ID = 20132910008 Lab Value = 0.029 Expected Conc. = 0.0304 Report level label = 0.022 Pct Recovery = 95% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = 052412 Laboratory ID = 20130650005 Lab Value = 0.033 Expected Conc. = 0.0304 Report level label = 0.022 Pct Recovery = 109% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl SpecificMix = 052412 Laboratory ID = 20140860102 Lab Value = 0.033 Expected Conc. = 0.0302 Report level label = 0.022 Pct Recovery = 109% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 012513 Laboratory ID = 20131920149 Lab Value = 0.035 Expected Conc. = 0.0302 Report level label = 0.022 Pct Recovery = 116% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl SpecificMix = 012513 Laboratory ID = 20131230084 Lab Value = 0.036 Expected Conc. = 0.03 Report level label = 0.022 Pct Recovery = 120% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl SpecificMix = 05BB029 Laboratory ID = 20130510051 Lab Value = 0.027 Expected Conc. = 0.03 Report level label = 0.022 Pct Recovery = 90% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl SpecificMix = 05BB029 Analysis Date = 02/08/18 Pct Recovery = 90% Analysis Date = 01/29/18 Pct Recovery = 90% Analysis Date = 01/29/18 Pct Recovery = 90% Analysis Date = 01/20/18 Pct Recovery = 90% Analysis Date = 01/20/18 Pct Recovery = 90% Analysis Date = 01/11/18 Pct Recovery = 90% Analysis Date = 01/11/18 Pct Recovery = 90% Analysis Date = 01/02/18 Pct Recovery = 90% Analysis Date = 01/02/18 Pct Recovery = 90% Analysis Date = 12/23/17 Pct Recovery = 90% Analysis Date = 12/23/17 Pct Recovery = 90% Analysis Date = 12/14/17 Pct Recovery = 90% Analysis Date = 12/14/17 Pct Recovery = 90% Analysis Date = 12/05/17 Pct Recovery = 90% Analysis Date = 12/05/17 Pct Recovery = 90% Analysis Date = 11/26/17 Pct Recovery = 90% Analysis Date = 11/26/17 Pct Recovery = 90% Analysis Date = 11/16/17 Pct Recovery = 90% Analysis Date = 11/16/17 Pct Recovery = 90% Analysis Date = 11/07/17 Pct Recovery = 90% Analysis Date = 11/07/17 Pct Recovery = 90% Analysis Date = 10/29/17 Pct Recovery = 90% Analysis Date = 10/29/17 Pct Recovery = 90% Analysis Date = 10/20/17 Pct Recovery = 89% Analysis Date = 10/20/17 Pct Recovery = 89% Analysis Date = 10/10/17 Pct Recovery = 89% Analysis Date = 10/10/17 Pct Recovery = 89% Analysis Date = 10/01/17 Pct Recovery = 89% Analysis Date = 10/01/17 Pct Recovery = 89% Analysis Date = 09/22/17 Pct Recovery = 89% Analysis Date = 09/22/17 Pct Recovery = 89% Analysis Date = 09/13/17 Pct Recovery = 89% Analysis Date = 09/13/17 Pct Recovery = 89% Analysis Date = 09/03/17 Pct Recovery = 89% Analysis Date = 09/03/17 Pct Recovery = 89% Analysis Date = 08/25/17 Pct Recovery = 89% Analysis Date = 08/25/17 Pct Recovery = 89% Analysis Date = 08/16/17 Pct Recovery = 89% Analysis Date = 08/16/17 Pct Recovery = 89% Analysis Date = 08/07/17 Pct Recovery = 89% Analysis Date = 08/07/17 Pct Recovery = 89% Analysis Date = 07/28/17 Pct Recovery = 89% Analysis Date = 07/28/17 Pct Recovery = 89% Analysis Date = 07/19/17 Pct Recovery = 89% Analysis Date = 07/19/17 Pct Recovery = 89% Analysis Date = 07/10/17 Pct Recovery = 89% Analysis Date = 07/10/17 Pct Recovery = 89% Analysis Date = 07/01/17 Pct Recovery = 89% Analysis Date = 07/01/17 Pct Recovery = 89% Analysis Date = 06/22/17 Pct Recovery = 89% Analysis Date = 06/22/17 Pct Recovery = 89% Analysis Date = 06/12/17 Pct Recovery = 89% Analysis Date = 06/12/17 Pct Recovery = 89% Analysis Date = 06/03/17 Pct Recovery = 89% Analysis Date = 06/03/17 Pct Recovery = 89% Analysis Date = 05/25/17 Pct Recovery = 89% Analysis Date = 05/25/17 Pct Recovery = 89% Analysis Date = 05/16/17 Pct Recovery = 89% Analysis Date = 05/16/17 Pct Recovery = 89% Analysis Date = 05/06/17 Pct Recovery = 89% Analysis Date = 05/06/17 Pct Recovery = 89% Analysis Date = 04/27/17 Pct Recovery = 89% Analysis Date = 04/27/17 Pct Recovery = 89% Analysis Date = 04/18/17 Pct Recovery = 89% Analysis Date = 04/18/17 Pct Recovery = 89% Analysis Date = 04/09/17 Pct Recovery = 89% Analysis Date = 04/09/17 Pct Recovery = 89% Analysis Date = 03/30/17 Pct Recovery = 89% Analysis Date = 03/30/17 Pct Recovery = 89% Analysis Date = 03/21/17 Pct Recovery = 89% Analysis Date = 03/21/17 Pct Recovery = 89% Analysis Date = 03/12/17 Pct Recovery = 88% Analysis Date = 03/12/17 Pct Recovery = 88% Analysis Date = 03/03/17 Pct Recovery = 88% Analysis Date = 03/03/17 Pct Recovery = 88% Analysis Date = 02/21/17 Pct Recovery = 88% Analysis Date = 02/21/17 Pct Recovery = 88% Analysis Date = 02/12/17 Pct Recovery = 88% Analysis Date = 02/12/17 Pct Recovery = 88% Analysis Date = 02/03/17 Pct Recovery = 88% Analysis Date = 02/03/17 Pct Recovery = 88% Analysis Date = 01/25/17 Pct Recovery = 88% Analysis Date = 01/25/17 Pct Recovery = 88% Analysis Date = 01/15/17 Pct Recovery = 88% Analysis Date = 01/15/17 Pct Recovery = 88% Analysis Date = 01/06/17 Pct Recovery = 88% Analysis Date = 01/06/17 Pct Recovery = 88% Analysis Date = 12/28/16 Pct Recovery = 88% Analysis Date = 12/28/16 Pct Recovery = 88% Analysis Date = 12/19/16 Pct Recovery = 88% Analysis Date = 12/19/16 Pct Recovery = 88% Analysis Date = 12/09/16 Pct Recovery = 88% Analysis Date = 12/09/16 Pct Recovery = 88% Analysis Date = 11/30/16 Pct Recovery = 88% Analysis Date = 11/30/16 Pct Recovery = 88% Analysis Date = 11/21/16 Pct Recovery = 88% Analysis Date = 11/21/16 Pct Recovery = 88% Analysis Date = 11/12/16 Pct Recovery = 88% Analysis Date = 11/12/16 Pct Recovery = 88% Analysis Date = 11/03/16 Pct Recovery = 88% Analysis Date = 11/03/16 Pct Recovery = 88% Analysis Date = 10/24/16 Pct Recovery = 88% Analysis Date = 10/24/16 Pct Recovery = 88% Analysis Date = 10/15/16 Pct Recovery = 88% Analysis Date = 10/15/16 Pct Recovery = 88% Analysis Date = 10/06/16 Pct Recovery = 88% Analysis Date = 10/06/16 Pct Recovery = 88% Analysis Date = 09/27/16 Pct Recovery = 88% Analysis Date = 09/27/16 Pct Recovery = 88% Analysis Date = 09/17/16 Pct Recovery = 88% Analysis Date = 09/17/16 Pct Recovery = 88% Analysis Date = 09/08/16 Pct Recovery = 88% Analysis Date = 09/08/16 Pct Recovery = 88% Analysis Date = 08/30/16 Pct Recovery = 88% Analysis Date = 08/30/16 Pct Recovery = 88% Analysis Date = 08/21/16 Pct Recovery = 88% Analysis Date = 08/21/16 Pct Recovery = 88% Analysis Date = 08/11/16 Pct Recovery = 88% Analysis Date = 08/11/16 Pct Recovery = 88% Analysis Date = 08/02/16 Pct Recovery = 88% Analysis Date = 08/02/16 Pct Recovery = 88% Analysis Date = 07/24/16 Pct Recovery = 88% Analysis Date = 07/24/16 Pct Recovery = 88% Analysis Date = 07/15/16 Pct Recovery = 88% Analysis Date = 07/15/16 Pct Recovery = 88% Analysis Date = 07/05/16 Pct Recovery = 89% Analysis Date = 07/05/16 Pct Recovery = 89% Analysis Date = 06/26/16 Pct Recovery = 89% Analysis Date = 06/26/16 Pct Recovery = 89% Analysis Date = 06/17/16 Pct Recovery = 89% Analysis Date = 06/17/16 Pct Recovery = 89% Analysis Date = 06/08/16 Pct Recovery = 89% Analysis Date = 06/08/16 Pct Recovery = 89% Analysis Date = 05/29/16 Pct Recovery = 89% Analysis Date = 05/29/16 Pct Recovery = 89% Analysis Date = 05/20/16 Pct Recovery = 89% Analysis Date = 05/20/16 Pct Recovery = 89% Analysis Date = 05/11/16 Pct Recovery = 89% Analysis Date = 05/11/16 Pct Recovery = 89% Analysis Date = 05/02/16 Pct Recovery = 89% Analysis Date = 05/02/16 Pct Recovery = 89% Analysis Date = 04/22/16 Pct Recovery = 89% Analysis Date = 04/22/16 Pct Recovery = 89% Analysis Date = 04/13/16 Pct Recovery = 89% Analysis Date = 04/13/16 Pct Recovery = 89% Analysis Date = 04/04/16 Pct Recovery = 89% Analysis Date = 04/04/16 Pct Recovery = 89% Analysis Date = 03/26/16 Pct Recovery = 89% Analysis Date = 03/26/16 Pct Recovery = 89% Analysis Date = 03/17/16 Pct Recovery = 89% Analysis Date = 03/17/16 Pct Recovery = 89% Analysis Date = 03/07/16 Pct Recovery = 89% Analysis Date = 03/07/16 Pct Recovery = 89% Analysis Date = 02/27/16 Pct Recovery = 89% Analysis Date = 02/27/16 Pct Recovery = 89% Analysis Date = 02/18/16 Pct Recovery = 90% Analysis Date = 02/18/16 Pct Recovery = 90% Analysis Date = 02/09/16 Pct Recovery = 90% Analysis Date = 02/09/16 Pct Recovery = 90% Analysis Date = 01/30/16 Pct Recovery = 90% Analysis Date = 01/30/16 Pct Recovery = 90% Analysis Date = 01/21/16 Pct Recovery = 90% Analysis Date = 01/21/16 Pct Recovery = 90% Analysis Date = 01/12/16 Pct Recovery = 90% Analysis Date = 01/12/16 Pct Recovery = 90% Analysis Date = 01/03/16 Pct Recovery = 90% Analysis Date = 01/03/16 Pct Recovery = 90% Analysis Date = 12/24/15 Pct Recovery = 91% Analysis Date = 12/24/15 Pct Recovery = 91% Analysis Date = 12/15/15 Pct Recovery = 91% Analysis Date = 12/15/15 Pct Recovery = 91% Analysis Date = 12/06/15 Pct Recovery = 91% Analysis Date = 12/06/15 Pct Recovery = 91% Analysis Date = 11/27/15 Pct Recovery = 91% Analysis Date = 11/27/15 Pct Recovery = 91% Analysis Date = 11/17/15 Pct Recovery = 92% Analysis Date = 11/17/15 Pct Recovery = 92% Analysis Date = 11/08/15 Pct Recovery = 92% Analysis Date = 11/08/15 Pct Recovery = 92% Analysis Date = 10/30/15 Pct Recovery = 92% Analysis Date = 10/30/15 Pct Recovery = 92% Analysis Date = 10/21/15 Pct Recovery = 92% Analysis Date = 10/21/15 Pct Recovery = 92% Analysis Date = 10/11/15 Pct Recovery = 92% Analysis Date = 10/11/15 Pct Recovery = 92% Analysis Date = 10/02/15 Pct Recovery = 93% Analysis Date = 10/02/15 Pct Recovery = 93% Analysis Date = 09/23/15 Pct Recovery = 93% Analysis Date = 09/23/15 Pct Recovery = 93% Analysis Date = 09/14/15 Pct Recovery = 93% Analysis Date = 09/14/15 Pct Recovery = 93% Analysis Date = 09/04/15 Pct Recovery = 93% Analysis Date = 09/04/15 Pct Recovery = 93% Analysis Date = 08/26/15 Pct Recovery = 94% Analysis Date = 08/26/15 Pct Recovery = 94% Analysis Date = 08/17/15 Pct Recovery = 94% Analysis Date = 08/17/15 Pct Recovery = 94% Analysis Date = 08/08/15 Pct Recovery = 94% Analysis Date = 08/08/15 Pct Recovery = 94% Analysis Date = 07/30/15 Pct Recovery = 94% Analysis Date = 07/30/15 Pct Recovery = 94% Analysis Date = 07/20/15 Pct Recovery = 94% Analysis Date = 07/20/15 Pct Recovery = 94% Analysis Date = 07/11/15 Pct Recovery = 95% Analysis Date = 07/11/15 Pct Recovery = 95% Analysis Date = 07/02/15 Pct Recovery = 95% Analysis Date = 07/02/15 Pct Recovery = 95% Analysis Date = 06/23/15 Pct Recovery = 95% Analysis Date = 06/23/15 Pct Recovery = 95% Analysis Date = 06/13/15 Pct Recovery = 96% Analysis Date = 06/13/15 Pct Recovery = 96% Analysis Date = 06/04/15 Pct Recovery = 96% Analysis Date = 06/04/15 Pct Recovery = 96% Analysis Date = 05/26/15 Pct Recovery = 96% Analysis Date = 05/26/15 Pct Recovery = 96% Analysis Date = 05/17/15 Pct Recovery = 96% Analysis Date = 05/17/15 Pct Recovery = 96% Analysis Date = 05/07/15 Pct Recovery = 97% Analysis Date = 05/07/15 Pct Recovery = 97% Analysis Date = 04/28/15 Pct Recovery = 97% Analysis Date = 04/28/15 Pct Recovery = 97% Analysis Date = 04/19/15 Pct Recovery = 97% Analysis Date = 04/19/15 Pct Recovery = 97% Analysis Date = 04/10/15 Pct Recovery = 98% Analysis Date = 04/10/15 Pct Recovery = 98% Analysis Date = 03/31/15 Pct Recovery = 98% Analysis Date = 03/31/15 Pct Recovery = 98% Analysis Date = 03/22/15 Pct Recovery = 98% Analysis Date = 03/22/15 Pct Recovery = 98% Analysis Date = 03/13/15 Pct Recovery = 99% Analysis Date = 03/13/15 Pct Recovery = 99% Analysis Date = 03/04/15 Pct Recovery = 99% Analysis Date = 03/04/15 Pct Recovery = 99% Analysis Date = 02/22/15 Pct Recovery = 99% Analysis Date = 02/22/15 Pct Recovery = 99% Analysis Date = 02/13/15 Pct Recovery = 100% Analysis Date = 02/13/15 Pct Recovery = 100% Analysis Date = 02/04/15 Pct Recovery = 100% Analysis Date = 02/04/15 Pct Recovery = 100% Analysis Date = 01/26/15 Pct Recovery = 100% Analysis Date = 01/26/15 Pct Recovery = 100% Analysis Date = 01/16/15 Pct Recovery = 101% Analysis Date = 01/16/15 Pct Recovery = 101% Analysis Date = 01/07/15 Pct Recovery = 101% Analysis Date = 01/07/15 Pct Recovery = 101% Analysis Date = 12/29/14 Pct Recovery = 101% Analysis Date = 12/29/14 Pct Recovery = 101% Analysis Date = 12/20/14 Pct Recovery = 102% Analysis Date = 12/20/14 Pct Recovery = 102% Analysis Date = 12/11/14 Pct Recovery = 102% Analysis Date = 12/11/14 Pct Recovery = 102% Analysis Date = 12/01/14 Pct Recovery = 102% Analysis Date = 12/01/14 Pct Recovery = 102% Analysis Date = 11/22/14 Pct Recovery = 102% Analysis Date = 11/22/14 Pct Recovery = 102% Analysis Date = 11/13/14 Pct Recovery = 102% Analysis Date = 11/13/14 Pct Recovery = 102% Analysis Date = 11/04/14 Pct Recovery = 102% Analysis Date = 11/04/14 Pct Recovery = 102% Analysis Date = 10/25/14 Pct Recovery = 102% Analysis Date = 10/25/14 Pct Recovery = 102% Analysis Date = 10/16/14 Pct Recovery = 103% Analysis Date = 10/16/14 Pct Recovery = 103% Analysis Date = 10/07/14 Pct Recovery = 103% Analysis Date = 10/07/14 Pct Recovery = 103% Analysis Date = 09/28/14 Pct Recovery = 103% Analysis Date = 09/28/14 Pct Recovery = 103% Analysis Date = 09/18/14 Pct Recovery = 103% Analysis Date = 09/18/14 Pct Recovery = 103% Analysis Date = 09/09/14 Pct Recovery = 103% Analysis Date = 09/09/14 Pct Recovery = 103% Analysis Date = 08/31/14 Pct Recovery = 103% Analysis Date = 08/31/14 Pct Recovery = 103% Analysis Date = 08/22/14 Pct Recovery = 103% Analysis Date = 08/22/14 Pct Recovery = 103% Analysis Date = 08/12/14 Pct Recovery = 103% Analysis Date = 08/12/14 Pct Recovery = 103% Analysis Date = 08/03/14 Pct Recovery = 103% Analysis Date = 08/03/14 Pct Recovery = 103% Analysis Date = 07/25/14 Pct Recovery = 103% Analysis Date = 07/25/14 Pct Recovery = 103% Analysis Date = 07/16/14 Pct Recovery = 103% Analysis Date = 07/16/14 Pct Recovery = 103% Analysis Date = 07/06/14 Pct Recovery = 103% Analysis Date = 07/06/14 Pct Recovery = 103% Analysis Date = 06/27/14 Pct Recovery = 103% Analysis Date = 06/27/14 Pct Recovery = 103% Analysis Date = 06/18/14 Pct Recovery = 103% Analysis Date = 06/18/14 Pct Recovery = 103% Analysis Date = 06/09/14 Pct Recovery = 103% Analysis Date = 06/09/14 Pct Recovery = 103% Analysis Date = 05/30/14 Pct Recovery = 103% Analysis Date = 05/30/14 Pct Recovery = 103% Analysis Date = 05/21/14 Pct Recovery = 104% Analysis Date = 05/21/14 Pct Recovery = 104% Analysis Date = 05/12/14 Pct Recovery = 104% Analysis Date = 05/12/14 Pct Recovery = 104% Analysis Date = 05/03/14 Pct Recovery = 104% Analysis Date = 05/03/14 Pct Recovery = 104% Analysis Date = 04/24/14 Pct Recovery = 104% Analysis Date = 04/24/14 Pct Recovery = 104% Analysis Date = 04/14/14 Pct Recovery = 104% Analysis Date = 04/14/14 Pct Recovery = 104% Analysis Date = 04/05/14 Pct Recovery = 104% Analysis Date = 04/05/14 Pct Recovery = 104% Analysis Date = 03/27/14 Pct Recovery = 104% Analysis Date = 03/27/14 Pct Recovery = 104% Analysis Date = 03/18/14 Pct Recovery = 104% Analysis Date = 03/18/14 Pct Recovery = 104% Analysis Date = 03/08/14 Pct Recovery = 104% Analysis Date = 03/08/14 Pct Recovery = 104% Analysis Date = 02/27/14 Pct Recovery = 105% Analysis Date = 02/27/14 Pct Recovery = 105% Analysis Date = 02/18/14 Pct Recovery = 105% Analysis Date = 02/18/14 Pct Recovery = 105% Analysis Date = 02/09/14 Pct Recovery = 105% Analysis Date = 02/09/14 Pct Recovery = 105% Analysis Date = 01/30/14 Pct Recovery = 105% Analysis Date = 01/30/14 Pct Recovery = 105% Analysis Date = 01/21/14 Pct Recovery = 105% Analysis Date = 01/21/14 Pct Recovery = 105% Analysis Date = 01/12/14 Pct Recovery = 105% Analysis Date = 01/12/14 Pct Recovery = 105% Analysis Date = 01/03/14 Pct Recovery = 105% Analysis Date = 01/03/14 Pct Recovery = 105% Analysis Date = 12/24/13 Pct Recovery = 105% Analysis Date = 12/24/13 Pct Recovery = 105% Analysis Date = 12/15/13 Pct Recovery = 105% Analysis Date = 12/15/13 Pct Recovery = 105% Analysis Date = 12/06/13 Pct Recovery = 105% Analysis Date = 12/06/13 Pct Recovery = 105% Analysis Date = 11/27/13 Pct Recovery = 105% Analysis Date = 11/27/13 Pct Recovery = 105% Analysis Date = 11/17/13 Pct Recovery = 105% Analysis Date = 11/17/13 Pct Recovery = 105% Analysis Date = 11/08/13 Pct Recovery = 105% Analysis Date = 11/08/13 Pct Recovery = 105% Analysis Date = 10/30/13 Pct Recovery = 105% Analysis Date = 10/30/13 Pct Recovery = 105% Analysis Date = 10/21/13 Pct Recovery = 105% Analysis Date = 10/21/13 Pct Recovery = 105% Analysis Date = 10/11/13 Pct Recovery = 105% Analysis Date = 10/11/13 Pct Recovery = 105% Analysis Date = 10/02/13 Pct Recovery = 105% Analysis Date = 10/02/13 Pct Recovery = 105% Analysis Date = 09/23/13 Pct Recovery = 105% Analysis Date = 09/23/13 Pct Recovery = 105% Analysis Date = 09/14/13 Pct Recovery = 105% Analysis Date = 09/14/13 Pct Recovery = 105% Analysis Date = 09/05/13 Pct Recovery = 105% Analysis Date = 09/05/13 Pct Recovery = 105% Analysis Date = 08/26/13 Pct Recovery = 106% Analysis Date = 08/26/13 Pct Recovery = 106% Analysis Date = 08/17/13 Pct Recovery = 106% Analysis Date = 08/17/13 Pct Recovery = 106% Analysis Date = 08/08/13 Pct Recovery = 106% Analysis Date = 08/08/13 Pct Recovery = 106% Analysis Date = 07/30/13 Pct Recovery = 106% Analysis Date = 07/30/13 Pct Recovery = 106% Analysis Date = 07/20/13 Pct Recovery = 106% Analysis Date = 07/20/13 Pct Recovery = 106% Analysis Date = 07/11/13 Pct Recovery = 106% Analysis Date = 07/11/13 Pct Recovery = 106% Analysis Date = 07/02/13 Pct Recovery = 106% Analysis Date = 07/02/13 Pct Recovery = 106% Analysis Date = 06/23/13 Pct Recovery = 106% Analysis Date = 06/23/13 Pct Recovery = 106% Analysis Date = 06/13/13 Pct Recovery = 106% Analysis Date = 06/13/13 Pct Recovery = 106% Analysis Date = 06/04/13 Pct Recovery = 106% Analysis Date = 06/04/13 Pct Recovery = 106% Analysis Date = 05/26/13 Pct Recovery = 106% Analysis Date = 05/26/13 Pct Recovery = 106% Analysis Date = 05/17/13 Pct Recovery = 106% Analysis Date = 05/17/13 Pct Recovery = 106% Analysis Date = 05/07/13 Pct Recovery = 106% Analysis Date = 05/07/13 Pct Recovery = 106% Analysis Date = 04/28/13 Pct Recovery = 106% Analysis Date = 04/28/13 Pct Recovery = 106% Analysis Date = 04/19/13 Pct Recovery = 106% Analysis Date = 04/19/13 Pct Recovery = 106% Analysis Date = 04/10/13 Pct Recovery = 106% Analysis Date = 04/10/13 Pct Recovery = 106% Analysis Date = 03/31/13 Pct Recovery = 106% Analysis Date = 03/31/13 Pct Recovery = 106% Analysis Date = 03/22/13 Pct Recovery = 106% Analysis Date = 03/22/13 Pct Recovery = 106% Analysis Date = 03/13/13 Pct Recovery = 106% Analysis Date = 03/13/13 Pct Recovery = 106% Analysis Date = 03/04/13 Pct Recovery = 106% Analysis Date = 03/04/13 Pct Recovery = 106% Analysis Date = 02/22/13 Pct Recovery = 106% Analysis Date = 02/22/13 Pct Recovery = 106% Analysis Date = 02/13/13 Pct Recovery = 106% Analysis Date = 02/13/13 Pct Recovery = 106% Analysis Date = 02/04/13 Pct Recovery = 106% Analysis Date = 02/04/13 Pct Recovery = 106% Analysis Date = 01/26/13 Pct Recovery = 106% Analysis Date = 01/26/13 Pct Recovery = 106% Analysis Date = 01/17/13 Pct Recovery = 106% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
MALAOXON

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 74 97% 23% 95% 26%
Total 74 97% 23% 95% 26%

Sample Statistics
MALAOXON

Characteristic N % % Basis
Plotted 74 99% Spiked
Estimated Values 4 5% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 1 1% Spiked
Spiked 75 .  
False Negatives 0 0% 0 out of 75
Not Spiked 43 .  
False Positives 1 2% 1 out of 43

OBSP Determination:
MALATHION
METHOD: 2033 , TESTIDCODE: 39532GCM35

Laboratory ID = 20132490342 Lab Value = 0.126 Expected Conc. = 0.15 Report level label = 0.016 Pct Recovery = 84% Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20172510330 Lab Value = 0.118 Expected Conc. = 0.107 Report level label = 0.016 Pct Recovery = 110% Analysis Date = 12/29/17 SpikeMix = ChemService 6537100: 100 µl & Abs 071817Pest: 100 µl SpecificMix = 071817Pest Laboratory ID = 20163370001 Lab Value = 0.089 Expected Conc. = 0.1 Report level label = 0.016 Pct Recovery = 89% Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl SpecificMix = B20160331 Laboratory ID = 20163150006 Lab Value = 0.087 Expected Conc. = 0.1 Report level label = 0.016 Pct Recovery = 87% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl SpecificMix = B20160331 Laboratory ID = 20161880109 Lab Value = 0.118 Expected Conc. = 0.099 Report level label = 0.016 Pct Recovery = 119% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl SpecificMix = 03FF076 Laboratory ID = 20152750006 Lab Value = 0.074 Expected Conc. = 0.096 Report level label = 0.016 Pct Recovery = 77% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl SpecificMix = EN150514012 Laboratory ID = 20152460215 Lab Value = 0.068 Expected Conc. = 0.096 Report level label = 0.016 Pct Recovery = 71% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl SpecificMix = EN150514012 Laboratory ID = 20171720140 Lab Value = 0.088 Expected Conc. = 0.08 Report level label = 0.016 Pct Recovery = 110% Analysis Date = 08/31/17 SpikeMix = Supelco LC20138V: 80 µl & Phenova B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20171660002 Lab Value = 0.082 Expected Conc. = 0.08 Report level label = 0.016 Pct Recovery = 103% Analysis Date = 08/23/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20170190026 Lab Value = 0.072 Expected Conc. = 0.08 Report level label = 0.016 Pct Recovery = 89% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20161470001 Lab Value = 0.084 Expected Conc. = 0.08 Report level label = 0.016 Pct Recovery = 105% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20170960001 Lab Value = 0.071 Expected Conc. = 0.0792 Report level label = 0.016 Pct Recovery = 90% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl SpecificMix = 03FF076 Laboratory ID = 20130940097 Lab Value = 0.055 Expected Conc. = 0.076 Report level label = 0.016 Pct Recovery = 72% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = 0507-12-04.2 Laboratory ID = 20123560092 Lab Value = 0.053 Expected Conc. = 0.076 Report level label = 0.016 Pct Recovery = 69% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = 0507-12-04.2 Laboratory ID = 20132140002 Lab Value = 0.073 Expected Conc. = 0.0752 Report level label = 0.016 Pct Recovery = 97% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl SpecificMix = LB99392 Laboratory ID = 20131370001 Lab Value = 0.090 Expected Conc. = 0.0752 Report level label = 0.016 Pct Recovery = 120% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl SpecificMix = LB99392 Laboratory ID = 20140370077 Lab Value = 0.055 Expected Conc. = 0.075 Report level label = 0.016 Pct Recovery = 73% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20132560001 Lab Value = 0.067 Expected Conc. = 0.075 Report level label = 0.016 Pct Recovery = 89% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20130810108 Lab Value = 0.055 Expected Conc. = 0.075 Report level label = 0.016 Pct Recovery = 73% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl SpecificMix = LB92783 Laboratory ID = 20130100066 Lab Value = 0.065 Expected Conc. = 0.075 Report level label = 0.016 Pct Recovery = 87% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl SpecificMix = LB92783 Laboratory ID = 20150430092 Lab Value = 0.048 Expected Conc. = 0.066 Report level label = 0.016 Pct Recovery = 73% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl SpecificMix = E1140407002 Laboratory ID = 20143110108 Lab Value = 0.058 Expected Conc. = 0.066 Report level label = 0.016 Pct Recovery = 88% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl SpecificMix = E1140407002 Laboratory ID = 20142720002 Lab Value = 0.050 Expected Conc. = 0.066 Report level label = 0.016 Pct Recovery = 76% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl SpecificMix = E1140407002 Laboratory ID = 20141770149 Lab Value = 0.049 Expected Conc. = 0.066 Report level label = 0.016 Pct Recovery = 75% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl SpecificMix = E1140407002 Laboratory ID = 20143240095 Lab Value = 0.063 Expected Conc. = 0.0648 Report level label = 0.016 Pct Recovery = 98% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl SpecificMix = 032714 Laboratory ID = 20142270001 Lab Value = 0.048 Expected Conc. = 0.0648 Report level label = 0.016 Pct Recovery = 74% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl SpecificMix = 032714 Laboratory ID = 20141220025 Lab Value = 0.076 Expected Conc. = 0.0648 Report level label = 0.016 Pct Recovery = 118% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl SpecificMix = 032714 Laboratory ID = 20172560101 Lab Value = 0.050 Expected Conc. = 0.055 Report level label = 0.016 Pct Recovery = 90% Analysis Date = 12/22/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6567600: 50 µl SpecificMix = 6567600 Laboratory ID = 20152330039 Lab Value = 0.036 Expected Conc. = 0.0484 Report level label = 0.016 Pct Recovery = 75% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl SpecificMix = 041415 Laboratory ID = 20151900132 Lab Value = 0.048 Expected Conc. = 0.0484 Report level label = 0.016 Pct Recovery = 99% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl SpecificMix = 041415 Laboratory ID = 20151270112 Lab Value = 0.044 Expected Conc. = 0.0484 Report level label = 0.016 Pct Recovery = 91% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl SpecificMix = 041415 Laboratory ID = 20153440001 Lab Value = 0.041 Expected Conc. = 0.048 Report level label = 0.016 Pct Recovery = 85% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = EN150514012 Laboratory ID = 20171160110 Lab Value = 0.036 Expected Conc. = 0.04 Report level label = 0.016 Pct Recovery = 90% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = B20160331 Laboratory ID = 20162380004 Lab Value = 0.034 Expected Conc. = 0.04 Report level label = 0.016 Pct Recovery = 86% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = B20160331 Laboratory ID = 20162150213 Lab Value = 0.037 Expected Conc. = 0.04 Report level label = 0.016 Pct Recovery = 91% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl SpecificMix = B20160331 Laboratory ID = 20172020035 Lab Value = 0.046 Expected Conc. = 0.0396 Report level label = 0.016 Pct Recovery = 116% Analysis Date = 11/07/17 SpikeMix = Abs 071717Pest: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20171510080 Lab Value = 0.040 Expected Conc. = 0.0396 Report level label = 0.016 Pct Recovery = 100% Analysis Date = 06/09/17 SpikeMix = Supelco LC20138V: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20170460061 Lab Value = 0.035 Expected Conc. = 0.0396 Report level label = 0.016 Pct Recovery = 89% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl SpecificMix = 03FF076 Laboratory ID = 20162660005 Lab Value = 0.037 Expected Conc. = 0.0396 Report level label = 0.016 Pct Recovery = 92% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl SpecificMix = 03FF076 Laboratory ID = 20161600087 Lab Value = 0.041 Expected Conc. = 0.0396 Report level label = 0.016 Pct Recovery = 104% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20161340228 Lab Value = 0.031 Expected Conc. = 0.0396 Report level label = 0.016 Pct Recovery = 78% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl SpecificMix = 03FF076 Laboratory ID = 20161190075 Lab Value = 0.029 Expected Conc. = 0.0396 Report level label = 0.016 Pct Recovery = 72% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20142470041 Lab Value = 0.031 Expected Conc. = 0.033 Report level label = 0.016 Pct Recovery = 93% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141910243 Lab Value = 0.022 Expected Conc. = 0.033 Report level label = 0.016 Pct Recovery = 67% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141640076 Lab Value = 0.033 Expected Conc. = 0.033 Report level label = 0.016 Pct Recovery = 100% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141360094 Lab Value = 0.026 Expected Conc. = 0.033 Report level label = 0.016 Pct Recovery = 78% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = E1140407002 Laboratory ID = 20150150115 Lab Value = 0.035 Expected Conc. = 0.0324 Report level label = 0.016 Pct Recovery = 107% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl SpecificMix = 032714 Laboratory ID = 20142820151 Lab Value = 0.026 Expected Conc. = 0.0324 Report level label = 0.016 Pct Recovery = 81% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl SpecificMix = 032714 Laboratory ID = 20141490205 Lab Value = 0.034 Expected Conc. = 0.0324 Report level label = 0.016 Pct Recovery = 104% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = 032714 Laboratory ID = 20141080004 Lab Value = 0.029 Expected Conc. = 0.0324 Report level label = 0.016 Pct Recovery = 89% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl SpecificMix = 032714 Laboratory ID = 20172780018 Lab Value = 0.036 Expected Conc. = 0.0321 Report level label = 0.016 Pct Recovery = 113% Analysis Date = 02/08/18 SpikeMix = ChemService 6537100: 30 µl & Abs 071817Pest: 30 µl SpecificMix = 071817Pest Laboratory ID = 20130510051 Lab Value = 0.025 Expected Conc. = 0.0304 Report level label = 0.016 Pct Recovery = 83% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl SpecificMix = 0507-12-04.2 Laboratory ID = 20140510043 Lab Value = 0.022 Expected Conc. = 0.0301 Report level label = 0.016 Pct Recovery = 74% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl SpecificMix = LB99392 Laboratory ID = 20133470008 Lab Value = 0.029 Expected Conc. = 0.0301 Report level label = 0.016 Pct Recovery = 95% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl SpecificMix = LB99392 Laboratory ID = 20133190012 Lab Value = 0.041 Expected Conc. = 0.0301 Report level label = 0.016 Pct Recovery = 136% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = LB99392 Laboratory ID = 20133050050 Lab Value = 0.040 Expected Conc. = 0.0301 Report level label = 0.016 Pct Recovery = 133% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl SpecificMix = LB99392 Laboratory ID = 20133580036 Lab Value = 0.020 Expected Conc. = 0.03 Report level label = 0.016 Pct Recovery = 66% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20131790009 Lab Value = 0.024 Expected Conc. = 0.03 Report level label = 0.016 Pct Recovery = 78% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20131510026 Lab Value = 0.023 Expected Conc. = 0.03 Report level label = 0.016 Pct Recovery = 76% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20130390105 Lab Value = 0.019 Expected Conc. = 0.03 Report level label = 0.016 Pct Recovery = 63% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl SpecificMix = LB92783 Laboratory ID = 20161050143 Lab Value = 0.022 Expected Conc. = 0.0242 Report level label = 0.016 Pct Recovery = 89% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 041415 Laboratory ID = 20152950078 Lab Value = 0.014 Expected Conc. = 0.0242 Report level label = 0.016 Pct Recovery = 59% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 041415 Laboratory ID = 20152040177 Lab Value = 0.029 Expected Conc. = 0.0242 Report level label = 0.016 Pct Recovery = 119% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl SpecificMix = 041415 Laboratory ID = 20151210037 Lab Value = 0.028 Expected Conc. = 0.0242 Report level label = 0.016 Pct Recovery = 114% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 041415 Laboratory ID = 20160070059 Lab Value = 0.024 Expected Conc. = 0.024 Report level label = 0.016 Pct Recovery = 100% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = EN150514012 Laboratory ID = 20153160001 Lab Value = 0.020 Expected Conc. = 0.024 Report level label = 0.016 Pct Recovery = 82% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = EN150514012 Laboratory ID = 20151760208 Lab Value = 0.037 Expected Conc. = 0.024 Report level label = 0.016 Pct Recovery = 156% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl SpecificMix = EN150514012 Laboratory ID = 20151480170 Lab Value = 0.027 Expected Conc. = 0.024 Report level label = 0.016 Pct Recovery = 111% Analysis Date = 06/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150514012 Analysis Date = 02/08/18 Pct Recovery = 104% Analysis Date = 01/29/18 Pct Recovery = 103% Analysis Date = 01/29/18 Pct Recovery = 103% Analysis Date = 01/20/18 Pct Recovery = 103% Analysis Date = 01/20/18 Pct Recovery = 103% Analysis Date = 01/11/18 Pct Recovery = 103% Analysis Date = 01/11/18 Pct Recovery = 103% Analysis Date = 01/02/18 Pct Recovery = 103% Analysis Date = 01/02/18 Pct Recovery = 103% Analysis Date = 12/23/17 Pct Recovery = 103% Analysis Date = 12/23/17 Pct Recovery = 103% Analysis Date = 12/14/17 Pct Recovery = 102% Analysis Date = 12/14/17 Pct Recovery = 102% Analysis Date = 12/05/17 Pct Recovery = 102% Analysis Date = 12/05/17 Pct Recovery = 102% Analysis Date = 11/26/17 Pct Recovery = 102% Analysis Date = 11/26/17 Pct Recovery = 102% Analysis Date = 11/16/17 Pct Recovery = 102% Analysis Date = 11/16/17 Pct Recovery = 102% Analysis Date = 11/07/17 Pct Recovery = 102% Analysis Date = 11/07/17 Pct Recovery = 102% Analysis Date = 10/29/17 Pct Recovery = 101% Analysis Date = 10/29/17 Pct Recovery = 101% Analysis Date = 10/20/17 Pct Recovery = 101% Analysis Date = 10/20/17 Pct Recovery = 101% Analysis Date = 10/10/17 Pct Recovery = 101% Analysis Date = 10/10/17 Pct Recovery = 101% Analysis Date = 10/01/17 Pct Recovery = 101% Analysis Date = 10/01/17 Pct Recovery = 101% Analysis Date = 09/22/17 Pct Recovery = 101% Analysis Date = 09/22/17 Pct Recovery = 101% Analysis Date = 09/13/17 Pct Recovery = 100% Analysis Date = 09/13/17 Pct Recovery = 100% Analysis Date = 09/03/17 Pct Recovery = 100% Analysis Date = 09/03/17 Pct Recovery = 100% Analysis Date = 08/25/17 Pct Recovery = 100% Analysis Date = 08/25/17 Pct Recovery = 100% Analysis Date = 08/16/17 Pct Recovery = 100% Analysis Date = 08/16/17 Pct Recovery = 100% Analysis Date = 08/07/17 Pct Recovery = 99% Analysis Date = 08/07/17 Pct Recovery = 99% Analysis Date = 07/28/17 Pct Recovery = 99% Analysis Date = 07/28/17 Pct Recovery = 99% Analysis Date = 07/19/17 Pct Recovery = 99% Analysis Date = 07/19/17 Pct Recovery = 99% Analysis Date = 07/10/17 Pct Recovery = 99% Analysis Date = 07/10/17 Pct Recovery = 99% Analysis Date = 07/01/17 Pct Recovery = 99% Analysis Date = 07/01/17 Pct Recovery = 99% Analysis Date = 06/21/17 Pct Recovery = 98% Analysis Date = 06/21/17 Pct Recovery = 98% Analysis Date = 06/12/17 Pct Recovery = 98% Analysis Date = 06/12/17 Pct Recovery = 98% Analysis Date = 06/03/17 Pct Recovery = 98% Analysis Date = 06/03/17 Pct Recovery = 98% Analysis Date = 05/25/17 Pct Recovery = 98% Analysis Date = 05/25/17 Pct Recovery = 98% Analysis Date = 05/15/17 Pct Recovery = 98% Analysis Date = 05/15/17 Pct Recovery = 98% Analysis Date = 05/06/17 Pct Recovery = 97% Analysis Date = 05/06/17 Pct Recovery = 97% Analysis Date = 04/27/17 Pct Recovery = 97% Analysis Date = 04/27/17 Pct Recovery = 97% Analysis Date = 04/18/17 Pct Recovery = 97% Analysis Date = 04/18/17 Pct Recovery = 97% Analysis Date = 04/08/17 Pct Recovery = 97% Analysis Date = 04/08/17 Pct Recovery = 97% Analysis Date = 03/30/17 Pct Recovery = 97% Analysis Date = 03/30/17 Pct Recovery = 97% Analysis Date = 03/21/17 Pct Recovery = 96% Analysis Date = 03/21/17 Pct Recovery = 96% Analysis Date = 03/12/17 Pct Recovery = 96% Analysis Date = 03/12/17 Pct Recovery = 96% Analysis Date = 03/02/17 Pct Recovery = 96% Analysis Date = 03/02/17 Pct Recovery = 96% Analysis Date = 02/21/17 Pct Recovery = 96% Analysis Date = 02/21/17 Pct Recovery = 96% Analysis Date = 02/12/17 Pct Recovery = 96% Analysis Date = 02/12/17 Pct Recovery = 96% Analysis Date = 02/03/17 Pct Recovery = 96% Analysis Date = 02/03/17 Pct Recovery = 96% Analysis Date = 01/24/17 Pct Recovery = 95% Analysis Date = 01/24/17 Pct Recovery = 95% Analysis Date = 01/15/17 Pct Recovery = 95% Analysis Date = 01/15/17 Pct Recovery = 95% Analysis Date = 01/06/17 Pct Recovery = 95% Analysis Date = 01/06/17 Pct Recovery = 95% Analysis Date = 12/28/16 Pct Recovery = 95% Analysis Date = 12/28/16 Pct Recovery = 95% Analysis Date = 12/18/16 Pct Recovery = 95% Analysis Date = 12/18/16 Pct Recovery = 95% Analysis Date = 12/09/16 Pct Recovery = 95% Analysis Date = 12/09/16 Pct Recovery = 95% Analysis Date = 11/30/16 Pct Recovery = 94% Analysis Date = 11/30/16 Pct Recovery = 94% Analysis Date = 11/21/16 Pct Recovery = 94% Analysis Date = 11/21/16 Pct Recovery = 94% Analysis Date = 11/11/16 Pct Recovery = 94% Analysis Date = 11/11/16 Pct Recovery = 94% Analysis Date = 11/02/16 Pct Recovery = 94% Analysis Date = 11/02/16 Pct Recovery = 94% Analysis Date = 10/24/16 Pct Recovery = 94% Analysis Date = 10/24/16 Pct Recovery = 94% Analysis Date = 10/15/16 Pct Recovery = 93% Analysis Date = 10/15/16 Pct Recovery = 93% Analysis Date = 10/05/16 Pct Recovery = 93% Analysis Date = 10/05/16 Pct Recovery = 93% Analysis Date = 09/26/16 Pct Recovery = 93% Analysis Date = 09/26/16 Pct Recovery = 93% Analysis Date = 09/17/16 Pct Recovery = 93% Analysis Date = 09/17/16 Pct Recovery = 93% Analysis Date = 09/08/16 Pct Recovery = 93% Analysis Date = 09/08/16 Pct Recovery = 93% Analysis Date = 08/29/16 Pct Recovery = 93% Analysis Date = 08/29/16 Pct Recovery = 93% Analysis Date = 08/20/16 Pct Recovery = 93% Analysis Date = 08/20/16 Pct Recovery = 93% Analysis Date = 08/11/16 Pct Recovery = 93% Analysis Date = 08/11/16 Pct Recovery = 93% Analysis Date = 08/02/16 Pct Recovery = 93% Analysis Date = 08/02/16 Pct Recovery = 93% Analysis Date = 07/23/16 Pct Recovery = 93% Analysis Date = 07/23/16 Pct Recovery = 93% Analysis Date = 07/14/16 Pct Recovery = 93% Analysis Date = 07/14/16 Pct Recovery = 93% Analysis Date = 07/05/16 Pct Recovery = 93% Analysis Date = 07/05/16 Pct Recovery = 93% Analysis Date = 06/26/16 Pct Recovery = 93% Analysis Date = 06/26/16 Pct Recovery = 93% Analysis Date = 06/16/16 Pct Recovery = 93% Analysis Date = 06/16/16 Pct Recovery = 93% Analysis Date = 06/07/16 Pct Recovery = 93% Analysis Date = 06/07/16 Pct Recovery = 93% Analysis Date = 05/29/16 Pct Recovery = 93% Analysis Date = 05/29/16 Pct Recovery = 93% Analysis Date = 05/20/16 Pct Recovery = 93% Analysis Date = 05/20/16 Pct Recovery = 93% Analysis Date = 05/10/16 Pct Recovery = 93% Analysis Date = 05/10/16 Pct Recovery = 93% Analysis Date = 05/01/16 Pct Recovery = 93% Analysis Date = 05/01/16 Pct Recovery = 93% Analysis Date = 04/22/16 Pct Recovery = 93% Analysis Date = 04/22/16 Pct Recovery = 93% Analysis Date = 04/13/16 Pct Recovery = 93% Analysis Date = 04/13/16 Pct Recovery = 93% Analysis Date = 04/03/16 Pct Recovery = 93% Analysis Date = 04/03/16 Pct Recovery = 93% Analysis Date = 03/25/16 Pct Recovery = 93% Analysis Date = 03/25/16 Pct Recovery = 93% Analysis Date = 03/16/16 Pct Recovery = 93% Analysis Date = 03/16/16 Pct Recovery = 93% Analysis Date = 03/07/16 Pct Recovery = 93% Analysis Date = 03/07/16 Pct Recovery = 93% Analysis Date = 02/26/16 Pct Recovery = 93% Analysis Date = 02/26/16 Pct Recovery = 93% Analysis Date = 02/17/16 Pct Recovery = 93% Analysis Date = 02/17/16 Pct Recovery = 93% Analysis Date = 02/08/16 Pct Recovery = 93% Analysis Date = 02/08/16 Pct Recovery = 93% Analysis Date = 01/30/16 Pct Recovery = 93% Analysis Date = 01/30/16 Pct Recovery = 93% Analysis Date = 01/20/16 Pct Recovery = 93% Analysis Date = 01/20/16 Pct Recovery = 93% Analysis Date = 01/11/16 Pct Recovery = 93% Analysis Date = 01/11/16 Pct Recovery = 93% Analysis Date = 01/02/16 Pct Recovery = 93% Analysis Date = 01/02/16 Pct Recovery = 93% Analysis Date = 12/24/15 Pct Recovery = 93% Analysis Date = 12/24/15 Pct Recovery = 93% Analysis Date = 12/14/15 Pct Recovery = 93% Analysis Date = 12/14/15 Pct Recovery = 93% Analysis Date = 12/05/15 Pct Recovery = 93% Analysis Date = 12/05/15 Pct Recovery = 93% Analysis Date = 11/26/15 Pct Recovery = 93% Analysis Date = 11/26/15 Pct Recovery = 93% Analysis Date = 11/17/15 Pct Recovery = 92% Analysis Date = 11/17/15 Pct Recovery = 92% Analysis Date = 11/07/15 Pct Recovery = 92% Analysis Date = 11/07/15 Pct Recovery = 92% Analysis Date = 10/29/15 Pct Recovery = 92% Analysis Date = 10/29/15 Pct Recovery = 92% Analysis Date = 10/20/15 Pct Recovery = 92% Analysis Date = 10/20/15 Pct Recovery = 92% Analysis Date = 10/11/15 Pct Recovery = 92% Analysis Date = 10/11/15 Pct Recovery = 92% Analysis Date = 10/01/15 Pct Recovery = 92% Analysis Date = 10/01/15 Pct Recovery = 92% Analysis Date = 09/22/15 Pct Recovery = 92% Analysis Date = 09/22/15 Pct Recovery = 92% Analysis Date = 09/13/15 Pct Recovery = 92% Analysis Date = 09/13/15 Pct Recovery = 92% Analysis Date = 09/04/15 Pct Recovery = 92% Analysis Date = 09/04/15 Pct Recovery = 92% Analysis Date = 08/25/15 Pct Recovery = 92% Analysis Date = 08/25/15 Pct Recovery = 92% Analysis Date = 08/16/15 Pct Recovery = 92% Analysis Date = 08/16/15 Pct Recovery = 92% Analysis Date = 08/07/15 Pct Recovery = 92% Analysis Date = 08/07/15 Pct Recovery = 92% Analysis Date = 07/29/15 Pct Recovery = 92% Analysis Date = 07/29/15 Pct Recovery = 92% Analysis Date = 07/19/15 Pct Recovery = 92% Analysis Date = 07/19/15 Pct Recovery = 92% Analysis Date = 07/10/15 Pct Recovery = 92% Analysis Date = 07/10/15 Pct Recovery = 92% Analysis Date = 07/01/15 Pct Recovery = 92% Analysis Date = 07/01/15 Pct Recovery = 92% Analysis Date = 06/22/15 Pct Recovery = 92% Analysis Date = 06/22/15 Pct Recovery = 92% Analysis Date = 06/12/15 Pct Recovery = 92% Analysis Date = 06/12/15 Pct Recovery = 92% Analysis Date = 06/03/15 Pct Recovery = 92% Analysis Date = 06/03/15 Pct Recovery = 92% Analysis Date = 05/25/15 Pct Recovery = 92% Analysis Date = 05/25/15 Pct Recovery = 92% Analysis Date = 05/16/15 Pct Recovery = 92% Analysis Date = 05/16/15 Pct Recovery = 92% Analysis Date = 05/06/15 Pct Recovery = 92% Analysis Date = 05/06/15 Pct Recovery = 92% Analysis Date = 04/27/15 Pct Recovery = 92% Analysis Date = 04/27/15 Pct Recovery = 92% Analysis Date = 04/18/15 Pct Recovery = 92% Analysis Date = 04/18/15 Pct Recovery = 92% Analysis Date = 04/09/15 Pct Recovery = 92% Analysis Date = 04/09/15 Pct Recovery = 92% Analysis Date = 03/30/15 Pct Recovery = 92% Analysis Date = 03/30/15 Pct Recovery = 92% Analysis Date = 03/21/15 Pct Recovery = 92% Analysis Date = 03/21/15 Pct Recovery = 92% Analysis Date = 03/12/15 Pct Recovery = 92% Analysis Date = 03/12/15 Pct Recovery = 92% Analysis Date = 03/03/15 Pct Recovery = 92% Analysis Date = 03/03/15 Pct Recovery = 92% Analysis Date = 02/21/15 Pct Recovery = 92% Analysis Date = 02/21/15 Pct Recovery = 92% Analysis Date = 02/12/15 Pct Recovery = 92% Analysis Date = 02/12/15 Pct Recovery = 92% Analysis Date = 02/03/15 Pct Recovery = 92% Analysis Date = 02/03/15 Pct Recovery = 92% Analysis Date = 01/25/15 Pct Recovery = 92% Analysis Date = 01/25/15 Pct Recovery = 92% Analysis Date = 01/15/15 Pct Recovery = 92% Analysis Date = 01/15/15 Pct Recovery = 92% Analysis Date = 01/06/15 Pct Recovery = 92% Analysis Date = 01/06/15 Pct Recovery = 92% Analysis Date = 12/28/14 Pct Recovery = 92% Analysis Date = 12/28/14 Pct Recovery = 92% Analysis Date = 12/19/14 Pct Recovery = 92% Analysis Date = 12/19/14 Pct Recovery = 92% Analysis Date = 12/09/14 Pct Recovery = 92% Analysis Date = 12/09/14 Pct Recovery = 92% Analysis Date = 11/30/14 Pct Recovery = 92% Analysis Date = 11/30/14 Pct Recovery = 92% Analysis Date = 11/21/14 Pct Recovery = 92% Analysis Date = 11/21/14 Pct Recovery = 92% Analysis Date = 11/12/14 Pct Recovery = 92% Analysis Date = 11/12/14 Pct Recovery = 92% Analysis Date = 11/02/14 Pct Recovery = 92% Analysis Date = 11/02/14 Pct Recovery = 92% Analysis Date = 10/24/14 Pct Recovery = 92% Analysis Date = 10/24/14 Pct Recovery = 92% Analysis Date = 10/15/14 Pct Recovery = 92% Analysis Date = 10/15/14 Pct Recovery = 92% Analysis Date = 10/06/14 Pct Recovery = 92% Analysis Date = 10/06/14 Pct Recovery = 92% Analysis Date = 09/26/14 Pct Recovery = 92% Analysis Date = 09/26/14 Pct Recovery = 92% Analysis Date = 09/17/14 Pct Recovery = 92% Analysis Date = 09/17/14 Pct Recovery = 92% Analysis Date = 09/08/14 Pct Recovery = 92% Analysis Date = 09/08/14 Pct Recovery = 92% Analysis Date = 08/30/14 Pct Recovery = 92% Analysis Date = 08/30/14 Pct Recovery = 92% Analysis Date = 08/20/14 Pct Recovery = 92% Analysis Date = 08/20/14 Pct Recovery = 92% Analysis Date = 08/11/14 Pct Recovery = 92% Analysis Date = 08/11/14 Pct Recovery = 92% Analysis Date = 08/02/14 Pct Recovery = 92% Analysis Date = 08/02/14 Pct Recovery = 92% Analysis Date = 07/24/14 Pct Recovery = 92% Analysis Date = 07/24/14 Pct Recovery = 92% Analysis Date = 07/14/14 Pct Recovery = 91% Analysis Date = 07/14/14 Pct Recovery = 91% Analysis Date = 07/05/14 Pct Recovery = 91% Analysis Date = 07/05/14 Pct Recovery = 91% Analysis Date = 06/26/14 Pct Recovery = 91% Analysis Date = 06/26/14 Pct Recovery = 91% Analysis Date = 06/17/14 Pct Recovery = 91% Analysis Date = 06/17/14 Pct Recovery = 91% Analysis Date = 06/07/14 Pct Recovery = 91% Analysis Date = 06/07/14 Pct Recovery = 91% Analysis Date = 05/29/14 Pct Recovery = 91% Analysis Date = 05/29/14 Pct Recovery = 91% Analysis Date = 05/20/14 Pct Recovery = 91% Analysis Date = 05/20/14 Pct Recovery = 91% Analysis Date = 05/11/14 Pct Recovery = 90% Analysis Date = 05/11/14 Pct Recovery = 90% Analysis Date = 05/01/14 Pct Recovery = 90% Analysis Date = 05/01/14 Pct Recovery = 90% Analysis Date = 04/22/14 Pct Recovery = 90% Analysis Date = 04/22/14 Pct Recovery = 90% Analysis Date = 04/13/14 Pct Recovery = 90% Analysis Date = 04/13/14 Pct Recovery = 90% Analysis Date = 04/04/14 Pct Recovery = 90% Analysis Date = 04/04/14 Pct Recovery = 90% Analysis Date = 03/25/14 Pct Recovery = 90% Analysis Date = 03/25/14 Pct Recovery = 90% Analysis Date = 03/16/14 Pct Recovery = 90% Analysis Date = 03/16/14 Pct Recovery = 90% Analysis Date = 03/07/14 Pct Recovery = 89% Analysis Date = 03/07/14 Pct Recovery = 89% Analysis Date = 02/26/14 Pct Recovery = 89% Analysis Date = 02/26/14 Pct Recovery = 89% Analysis Date = 02/16/14 Pct Recovery = 89% Analysis Date = 02/16/14 Pct Recovery = 89% Analysis Date = 02/07/14 Pct Recovery = 89% Analysis Date = 02/07/14 Pct Recovery = 89% Analysis Date = 01/29/14 Pct Recovery = 89% Analysis Date = 01/29/14 Pct Recovery = 89% Analysis Date = 01/20/14 Pct Recovery = 89% Analysis Date = 01/20/14 Pct Recovery = 89% Analysis Date = 01/10/14 Pct Recovery = 89% Analysis Date = 01/10/14 Pct Recovery = 89% Analysis Date = 01/01/14 Pct Recovery = 88% Analysis Date = 01/01/14 Pct Recovery = 88% Analysis Date = 12/23/13 Pct Recovery = 88% Analysis Date = 12/23/13 Pct Recovery = 88% Analysis Date = 12/14/13 Pct Recovery = 88% Analysis Date = 12/14/13 Pct Recovery = 88% Analysis Date = 12/04/13 Pct Recovery = 88% Analysis Date = 12/04/13 Pct Recovery = 88% Analysis Date = 11/25/13 Pct Recovery = 88% Analysis Date = 11/25/13 Pct Recovery = 88% Analysis Date = 11/16/13 Pct Recovery = 88% Analysis Date = 11/16/13 Pct Recovery = 88% Analysis Date = 11/07/13 Pct Recovery = 88% Analysis Date = 11/07/13 Pct Recovery = 88% Analysis Date = 10/28/13 Pct Recovery = 88% Analysis Date = 10/28/13 Pct Recovery = 88% Analysis Date = 10/19/13 Pct Recovery = 87% Analysis Date = 10/19/13 Pct Recovery = 87% Analysis Date = 10/10/13 Pct Recovery = 87% Analysis Date = 10/10/13 Pct Recovery = 87% Analysis Date = 10/01/13 Pct Recovery = 87% Analysis Date = 10/01/13 Pct Recovery = 87% Analysis Date = 09/21/13 Pct Recovery = 87% Analysis Date = 09/21/13 Pct Recovery = 87% Analysis Date = 09/12/13 Pct Recovery = 87% Analysis Date = 09/12/13 Pct Recovery = 87% Analysis Date = 09/03/13 Pct Recovery = 87% Analysis Date = 09/03/13 Pct Recovery = 87% Analysis Date = 08/25/13 Pct Recovery = 87% Analysis Date = 08/25/13 Pct Recovery = 87% Analysis Date = 08/15/13 Pct Recovery = 86% Analysis Date = 08/15/13 Pct Recovery = 86% Analysis Date = 08/06/13 Pct Recovery = 86% Analysis Date = 08/06/13 Pct Recovery = 86% Analysis Date = 07/28/13 Pct Recovery = 86% Analysis Date = 07/28/13 Pct Recovery = 86% Analysis Date = 07/19/13 Pct Recovery = 86% Analysis Date = 07/19/13 Pct Recovery = 86% Analysis Date = 07/09/13 Pct Recovery = 86% Analysis Date = 07/09/13 Pct Recovery = 86% Analysis Date = 06/30/13 Pct Recovery = 86% Analysis Date = 06/30/13 Pct Recovery = 86% Analysis Date = 06/21/13 Pct Recovery = 86% Analysis Date = 06/21/13 Pct Recovery = 86% Analysis Date = 06/12/13 Pct Recovery = 85% Analysis Date = 06/12/13 Pct Recovery = 85% Analysis Date = 06/02/13 Pct Recovery = 85% Analysis Date = 06/02/13 Pct Recovery = 85% Analysis Date = 05/24/13 Pct Recovery = 85% Analysis Date = 05/24/13 Pct Recovery = 85% Analysis Date = 05/15/13 Pct Recovery = 85% Analysis Date = 05/15/13 Pct Recovery = 85% Analysis Date = 05/06/13 Pct Recovery = 85% Analysis Date = 05/06/13 Pct Recovery = 85% Analysis Date = 04/26/13 Pct Recovery = 85% Analysis Date = 04/26/13 Pct Recovery = 85% Analysis Date = 04/17/13 Pct Recovery = 85% Analysis Date = 04/17/13 Pct Recovery = 85% Analysis Date = 04/08/13 Pct Recovery = 84% Analysis Date = 04/08/13 Pct Recovery = 84% Analysis Date = 03/30/13 Pct Recovery = 84% Analysis Date = 03/30/13 Pct Recovery = 84% Analysis Date = 03/20/13 Pct Recovery = 84% Analysis Date = 03/20/13 Pct Recovery = 84% Analysis Date = 03/11/13 Pct Recovery = 84% Analysis Date = 03/11/13 Pct Recovery = 84% Analysis Date = 03/02/13 Pct Recovery = 84% Analysis Date = 03/02/13 Pct Recovery = 84% Analysis Date = 02/21/13 Pct Recovery = 84% Analysis Date = 02/21/13 Pct Recovery = 84% Analysis Date = 02/11/13 Pct Recovery = 84% Analysis Date = 02/11/13 Pct Recovery = 84% Analysis Date = 02/02/13 Pct Recovery = 83% Analysis Date = 02/02/13 Pct Recovery = 83% Analysis Date = 01/24/13 Pct Recovery = 83% Analysis Date = 01/24/13 Pct Recovery = 83% Analysis Date = 01/15/13 Pct Recovery = 83% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
MALATHION

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 68 92% 19% 89% 20%
Total 68 92% 19% 89% 20%

Sample Statistics
MALATHION

Characteristic N % % Basis
Plotted 68 96% Spiked
Estimated Values 2 3% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 71 .  
False Negatives 3 4% 3 out of 71
Not Spiked 47 .  
False Positives 0 0% 0 out of 47

OBSP Determination:
METALAXYL
METHOD: 2033 , TESTIDCODE: 61596GCM39

Laboratory ID = 20132490342 Lab Value = 0.269 Expected Conc. = 0.276 Report level label = 0.014 Pct Recovery = 97% Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20140370077 Lab Value = 0.109 Expected Conc. = 0.138 Report level label = 0.014 Pct Recovery = 79% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20132560001 Lab Value = 0.139 Expected Conc. = 0.138 Report level label = 0.014 Pct Recovery = 101% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20132140002 Lab Value = 0.143 Expected Conc. = 0.1376 Report level label = 0.014 Pct Recovery = 104% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl SpecificMix = LB99392 Laboratory ID = 20131370001 Lab Value = 0.140 Expected Conc. = 0.1376 Report level label = 0.014 Pct Recovery = 102% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl SpecificMix = LB99392 Laboratory ID = 20172510330 Lab Value = 0.086 Expected Conc. = 0.093 Report level label = 0.014 Pct Recovery = 93% Analysis Date = 12/29/17 SpikeMix = ChemService 6537100: 100 µl & Abs 071817Pest: 100 µl SpecificMix = 6537100 Laboratory ID = 20162860079 Lab Value = 0.096 Expected Conc. = 0.09 Report level label = 0.014 Pct Recovery = 107% Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl SpecificMix = 5054800 Laboratory ID = 20161880109 Lab Value = 0.113 Expected Conc. = 0.09 Report level label = 0.014 Pct Recovery = 126% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl SpecificMix = 5054800 Laboratory ID = 20163370001 Lab Value = 0.085 Expected Conc. = 0.0875 Report level label = 0.014 Pct Recovery = 97% Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl SpecificMix = LC20138V Laboratory ID = 20152750006 Lab Value = 0.085 Expected Conc. = 0.084 Report level label = 0.014 Pct Recovery = 102% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl SpecificMix = EN150514012 Laboratory ID = 20152460215 Lab Value = 0.071 Expected Conc. = 0.084 Report level label = 0.014 Pct Recovery = 85% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl SpecificMix = EN150514012 Laboratory ID = 20130940097 Lab Value = 0.063 Expected Conc. = 0.077 Report level label = 0.014 Pct Recovery = 82% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = 0507-12-04.2 Laboratory ID = 20123560092 Lab Value = 0.063 Expected Conc. = 0.077 Report level label = 0.014 Pct Recovery = 82% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = 0507-12-04.2 Laboratory ID = 20130810108 Lab Value = 0.067 Expected Conc. = 0.075 Report level label = 0.014 Pct Recovery = 90% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl SpecificMix = LB92783 Laboratory ID = 20130100066 Lab Value = 0.071 Expected Conc. = 0.075 Report level label = 0.014 Pct Recovery = 95% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl SpecificMix = LB92783 Laboratory ID = 20171380001 Lab Value = 0.054 Expected Conc. = 0.072 Report level label = 0.014 Pct Recovery = 74% Analysis Date = 06/07/17 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 5054800 Laboratory ID = 20170960001 Lab Value = 0.065 Expected Conc. = 0.072 Report level label = 0.014 Pct Recovery = 91% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl SpecificMix = 5054800 Laboratory ID = 20161740258 Lab Value = 0.052 Expected Conc. = 0.072 Report level label = 0.014 Pct Recovery = 72% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 5054800 Laboratory ID = 20171720140 Lab Value = 0.078 Expected Conc. = 0.07 Report level label = 0.014 Pct Recovery = 112% Analysis Date = 08/31/17 SpikeMix = Supelco LC20138V: 80 µl & Phenova B20160331: 80 µl SpecificMix = LC20138V Laboratory ID = 20170740063 Lab Value = 0.063 Expected Conc. = 0.07 Report level label = 0.014 Pct Recovery = 89% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl SpecificMix = LC20138V Laboratory ID = 20161470001 Lab Value = 0.074 Expected Conc. = 0.07 Report level label = 0.014 Pct Recovery = 106% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl SpecificMix = LC20138V Laboratory ID = 20143240095 Lab Value = 0.059 Expected Conc. = 0.0564 Report level label = 0.014 Pct Recovery = 104% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl SpecificMix = 032714 Laboratory ID = 20142270001 Lab Value = 0.040 Expected Conc. = 0.0564 Report level label = 0.014 Pct Recovery = 71% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl SpecificMix = 032714 Laboratory ID = 20141220025 Lab Value = 0.067 Expected Conc. = 0.0564 Report level label = 0.014 Pct Recovery = 118% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl SpecificMix = 032714 Laboratory ID = 20150430092 Lab Value = 0.041 Expected Conc. = 0.0559 Report level label = 0.014 Pct Recovery = 74% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl SpecificMix = E1140407002 Laboratory ID = 20143110108 Lab Value = 0.042 Expected Conc. = 0.0559 Report level label = 0.014 Pct Recovery = 76% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl SpecificMix = E1140407002 Laboratory ID = 20142720002 Lab Value = 0.044 Expected Conc. = 0.0559 Report level label = 0.014 Pct Recovery = 79% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl SpecificMix = E1140407002 Laboratory ID = 20141770149 Lab Value = 0.047 Expected Conc. = 0.0559 Report level label = 0.014 Pct Recovery = 83% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl SpecificMix = E1140407002 Laboratory ID = 20133580036 Lab Value = 0.043 Expected Conc. = 0.0552 Report level label = 0.014 Pct Recovery = 77% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20131790009 Lab Value = 0.038 Expected Conc. = 0.0552 Report level label = 0.014 Pct Recovery = 69% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20131510026 Lab Value = 0.046 Expected Conc. = 0.0552 Report level label = 0.014 Pct Recovery = 83% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20140510043 Lab Value = 0.042 Expected Conc. = 0.055 Report level label = 0.014 Pct Recovery = 77% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl SpecificMix = LB99392 Laboratory ID = 20133470008 Lab Value = 0.056 Expected Conc. = 0.055 Report level label = 0.014 Pct Recovery = 101% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl SpecificMix = LB99392 Laboratory ID = 20133190012 Lab Value = 0.056 Expected Conc. = 0.055 Report level label = 0.014 Pct Recovery = 102% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = LB99392 Laboratory ID = 20133050050 Lab Value = 0.052 Expected Conc. = 0.055 Report level label = 0.014 Pct Recovery = 94% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl SpecificMix = LB99392 Laboratory ID = 20172370001 Lab Value = 0.040 Expected Conc. = 0.0465 Report level label = 0.014 Pct Recovery = 86% Analysis Date = 11/18/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6537100: 50 µl SpecificMix = 6537100 Laboratory ID = 20172230001 Lab Value = 0.055 Expected Conc. = 0.0465 Report level label = 0.014 Pct Recovery = 119% Analysis Date = 10/19/17 SpikeMix = ChemService 6472100: 50 µl & Abs 071717Pest: 50 µl SpecificMix = 071717Pest Laboratory ID = 20160630046 Lab Value = 0.031 Expected Conc. = 0.042 Report level label = 0.014 Pct Recovery = 73% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = EN150514012 Laboratory ID = 20153440001 Lab Value = 0.031 Expected Conc. = 0.042 Report level label = 0.014 Pct Recovery = 73% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = EN150514012 Laboratory ID = 20152330039 Lab Value = 0.030 Expected Conc. = 0.042 Report level label = 0.014 Pct Recovery = 71% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl SpecificMix = 041415 Laboratory ID = 20151900132 Lab Value = 0.048 Expected Conc. = 0.042 Report level label = 0.014 Pct Recovery = 115% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl SpecificMix = 041415 Laboratory ID = 20151270112 Lab Value = 0.040 Expected Conc. = 0.042 Report level label = 0.014 Pct Recovery = 94% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl SpecificMix = 041415 Laboratory ID = 20172020035 Lab Value = 0.047 Expected Conc. = 0.0372 Report level label = 0.014 Pct Recovery = 125% Analysis Date = 11/07/17 SpikeMix = Abs 071717Pest: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 071717Pest Laboratory ID = 20171940002 Lab Value = 0.032 Expected Conc. = 0.036 Report level label = 0.014 Pct Recovery = 89% Analysis Date = 11/10/17 SpikeMix = ChemService 5054800: 40 µl & NSI 041816: 40 µl SpecificMix = 5054800 Laboratory ID = 20170460061 Lab Value = 0.032 Expected Conc. = 0.036 Report level label = 0.014 Pct Recovery = 89% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl SpecificMix = 5054800 Laboratory ID = 20163560019 Lab Value = 0.033 Expected Conc. = 0.036 Report level label = 0.014 Pct Recovery = 93% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl SpecificMix = 5054800 Laboratory ID = 20162150213 Lab Value = 0.032 Expected Conc. = 0.036 Report level label = 0.014 Pct Recovery = 89% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl SpecificMix = 5054800 Laboratory ID = 20171510080 Lab Value = 0.037 Expected Conc. = 0.035 Report level label = 0.014 Pct Recovery = 106% Analysis Date = 06/09/17 SpikeMix = Supelco LC20138V: 40 µl & Crescent 03FF076: 40 µl SpecificMix = LC20138V Laboratory ID = 20162520001 Lab Value = 0.041 Expected Conc. = 0.035 Report level label = 0.014 Pct Recovery = 118% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl SpecificMix = LC20138V Laboratory ID = 20162660005 Lab Value = 0.031 Expected Conc. = 0.035 Report level label = 0.014 Pct Recovery = 87% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl SpecificMix = LC20138V Laboratory ID = 20162020124 Lab Value = 0.032 Expected Conc. = 0.035 Report level label = 0.014 Pct Recovery = 90% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl SpecificMix = LC20138V Laboratory ID = 20130510051 Lab Value = 0.026 Expected Conc. = 0.0308 Report level label = 0.014 Pct Recovery = 83% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl SpecificMix = 0507-12-04.2 Laboratory ID = 20130390105 Lab Value = 0.022 Expected Conc. = 0.03 Report level label = 0.014 Pct Recovery = 72% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl SpecificMix = LB92783 Laboratory ID = 20150150115 Lab Value = 0.022 Expected Conc. = 0.0282 Report level label = 0.014 Pct Recovery = 78% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl SpecificMix = 032714 Laboratory ID = 20142820151 Lab Value = 0.026 Expected Conc. = 0.0282 Report level label = 0.014 Pct Recovery = 90% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl SpecificMix = 032714 Laboratory ID = 20141490205 Lab Value = 0.028 Expected Conc. = 0.0282 Report level label = 0.014 Pct Recovery = 98% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = 032714 Laboratory ID = 20141080004 Lab Value = 0.025 Expected Conc. = 0.0282 Report level label = 0.014 Pct Recovery = 89% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl SpecificMix = 032714 Laboratory ID = 20142470041 Lab Value = 0.033 Expected Conc. = 0.0279 Report level label = 0.014 Pct Recovery = 119% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141910243 Lab Value = 0.019 Expected Conc. = 0.0279 Report level label = 0.014 Pct Recovery = 69% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141640076 Lab Value = 0.023 Expected Conc. = 0.0279 Report level label = 0.014 Pct Recovery = 81% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141360094 Lab Value = 0.023 Expected Conc. = 0.0279 Report level label = 0.014 Pct Recovery = 81% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = E1140407002 Laboratory ID = 20173120093 Lab Value = 0.032 Expected Conc. = 0.0279 Report level label = 0.014 Pct Recovery = 114% Analysis Date = 03/10/18 SpikeMix = ChemService 6472100: 30 µl & ChemService 6537100: 30 µl SpecificMix = 6537100 Laboratory ID = 20172780018 Lab Value = 0.022 Expected Conc. = 0.0279 Report level label = 0.014 Pct Recovery = 80% Analysis Date = 02/08/18 SpikeMix = ChemService 6537100: 30 µl & Abs 071817Pest: 30 µl SpecificMix = 6537100 Laboratory ID = 20161050143 Lab Value = 0.020 Expected Conc. = 0.021 Report level label = 0.014 Pct Recovery = 96% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 041415 Laboratory ID = 20160560044 Lab Value = 0.016 Expected Conc. = 0.021 Report level label = 0.014 Pct Recovery = 76% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl SpecificMix = 041415 Laboratory ID = 20160210080 Lab Value = 0.019 Expected Conc. = 0.021 Report level label = 0.014 Pct Recovery = 92% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 041415 Laboratory ID = 20160070059 Lab Value = 0.019 Expected Conc. = 0.021 Report level label = 0.014 Pct Recovery = 88% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = EN150514012 Laboratory ID = 20153160001 Lab Value = 0.016 Expected Conc. = 0.021 Report level label = 0.014 Pct Recovery = 78% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = EN150514012 Laboratory ID = 20152950078 Lab Value = 0.012 Expected Conc. = 0.021 Report level label = 0.014 Pct Recovery = 57% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 041415 Laboratory ID = 20152040177 Lab Value = 0.028 Expected Conc. = 0.021 Report level label = 0.014 Pct Recovery = 131% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl SpecificMix = 041415 Laboratory ID = 20151760208 Lab Value = 0.031 Expected Conc. = 0.021 Report level label = 0.014 Pct Recovery = 149% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl SpecificMix = EN150514012 Laboratory ID = 20151480170 Lab Value = 0.020 Expected Conc. = 0.021 Report level label = 0.014 Pct Recovery = 94% Analysis Date = 06/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150514012 Laboratory ID = 20151210037 Lab Value = 0.021 Expected Conc. = 0.021 Report level label = 0.014 Pct Recovery = 101% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 041415 Analysis Date = 03/10/18 Pct Recovery = 102% Analysis Date = 02/28/18 Pct Recovery = 102% Analysis Date = 02/28/18 Pct Recovery = 102% Analysis Date = 02/19/18 Pct Recovery = 102% Analysis Date = 02/19/18 Pct Recovery = 102% Analysis Date = 02/09/18 Pct Recovery = 102% Analysis Date = 02/09/18 Pct Recovery = 102% Analysis Date = 01/31/18 Pct Recovery = 102% Analysis Date = 01/31/18 Pct Recovery = 102% Analysis Date = 01/22/18 Pct Recovery = 101% Analysis Date = 01/22/18 Pct Recovery = 101% Analysis Date = 01/12/18 Pct Recovery = 101% Analysis Date = 01/12/18 Pct Recovery = 101% Analysis Date = 01/03/18 Pct Recovery = 101% Analysis Date = 01/03/18 Pct Recovery = 101% Analysis Date = 12/24/17 Pct Recovery = 101% Analysis Date = 12/24/17 Pct Recovery = 101% Analysis Date = 12/15/17 Pct Recovery = 101% Analysis Date = 12/15/17 Pct Recovery = 101% Analysis Date = 12/06/17 Pct Recovery = 101% Analysis Date = 12/06/17 Pct Recovery = 101% Analysis Date = 11/26/17 Pct Recovery = 100% Analysis Date = 11/26/17 Pct Recovery = 100% Analysis Date = 11/17/17 Pct Recovery = 100% Analysis Date = 11/17/17 Pct Recovery = 100% Analysis Date = 11/07/17 Pct Recovery = 100% Analysis Date = 11/07/17 Pct Recovery = 100% Analysis Date = 10/29/17 Pct Recovery = 100% Analysis Date = 10/29/17 Pct Recovery = 100% Analysis Date = 10/20/17 Pct Recovery = 100% Analysis Date = 10/20/17 Pct Recovery = 100% Analysis Date = 10/10/17 Pct Recovery = 100% Analysis Date = 10/10/17 Pct Recovery = 100% Analysis Date = 10/01/17 Pct Recovery = 99% Analysis Date = 10/01/17 Pct Recovery = 99% Analysis Date = 09/21/17 Pct Recovery = 99% Analysis Date = 09/21/17 Pct Recovery = 99% Analysis Date = 09/12/17 Pct Recovery = 99% Analysis Date = 09/12/17 Pct Recovery = 99% Analysis Date = 09/03/17 Pct Recovery = 99% Analysis Date = 09/03/17 Pct Recovery = 99% Analysis Date = 08/24/17 Pct Recovery = 99% Analysis Date = 08/24/17 Pct Recovery = 99% Analysis Date = 08/15/17 Pct Recovery = 99% Analysis Date = 08/15/17 Pct Recovery = 99% Analysis Date = 08/05/17 Pct Recovery = 98% Analysis Date = 08/05/17 Pct Recovery = 98% Analysis Date = 07/27/17 Pct Recovery = 98% Analysis Date = 07/27/17 Pct Recovery = 98% Analysis Date = 07/18/17 Pct Recovery = 98% Analysis Date = 07/18/17 Pct Recovery = 98% Analysis Date = 07/08/17 Pct Recovery = 98% Analysis Date = 07/08/17 Pct Recovery = 98% Analysis Date = 06/29/17 Pct Recovery = 98% Analysis Date = 06/29/17 Pct Recovery = 98% Analysis Date = 06/19/17 Pct Recovery = 98% Analysis Date = 06/19/17 Pct Recovery = 98% Analysis Date = 06/10/17 Pct Recovery = 97% Analysis Date = 06/10/17 Pct Recovery = 97% Analysis Date = 06/01/17 Pct Recovery = 97% Analysis Date = 06/01/17 Pct Recovery = 97% Analysis Date = 05/22/17 Pct Recovery = 97% Analysis Date = 05/22/17 Pct Recovery = 97% Analysis Date = 05/13/17 Pct Recovery = 97% Analysis Date = 05/13/17 Pct Recovery = 97% Analysis Date = 05/03/17 Pct Recovery = 97% Analysis Date = 05/03/17 Pct Recovery = 97% Analysis Date = 04/24/17 Pct Recovery = 97% Analysis Date = 04/24/17 Pct Recovery = 97% Analysis Date = 04/15/17 Pct Recovery = 96% Analysis Date = 04/15/17 Pct Recovery = 96% Analysis Date = 04/05/17 Pct Recovery = 96% Analysis Date = 04/05/17 Pct Recovery = 96% Analysis Date = 03/27/17 Pct Recovery = 96% Analysis Date = 03/27/17 Pct Recovery = 96% Analysis Date = 03/17/17 Pct Recovery = 96% Analysis Date = 03/17/17 Pct Recovery = 96% Analysis Date = 03/08/17 Pct Recovery = 96% Analysis Date = 03/08/17 Pct Recovery = 96% Analysis Date = 02/27/17 Pct Recovery = 96% Analysis Date = 02/27/17 Pct Recovery = 96% Analysis Date = 02/17/17 Pct Recovery = 96% Analysis Date = 02/17/17 Pct Recovery = 96% Analysis Date = 02/08/17 Pct Recovery = 95% Analysis Date = 02/08/17 Pct Recovery = 95% Analysis Date = 01/29/17 Pct Recovery = 95% Analysis Date = 01/29/17 Pct Recovery = 95% Analysis Date = 01/20/17 Pct Recovery = 95% Analysis Date = 01/20/17 Pct Recovery = 95% Analysis Date = 01/11/17 Pct Recovery = 95% Analysis Date = 01/11/17 Pct Recovery = 95% Analysis Date = 01/01/17 Pct Recovery = 95% Analysis Date = 01/01/17 Pct Recovery = 95% Analysis Date = 12/23/16 Pct Recovery = 95% Analysis Date = 12/23/16 Pct Recovery = 95% Analysis Date = 12/13/16 Pct Recovery = 95% Analysis Date = 12/13/16 Pct Recovery = 95% Analysis Date = 12/04/16 Pct Recovery = 94% Analysis Date = 12/04/16 Pct Recovery = 94% Analysis Date = 11/25/16 Pct Recovery = 94% Analysis Date = 11/25/16 Pct Recovery = 94% Analysis Date = 11/15/16 Pct Recovery = 94% Analysis Date = 11/15/16 Pct Recovery = 94% Analysis Date = 11/06/16 Pct Recovery = 94% Analysis Date = 11/06/16 Pct Recovery = 94% Analysis Date = 10/27/16 Pct Recovery = 94% Analysis Date = 10/27/16 Pct Recovery = 94% Analysis Date = 10/18/16 Pct Recovery = 94% Analysis Date = 10/18/16 Pct Recovery = 94% Analysis Date = 10/09/16 Pct Recovery = 94% Analysis Date = 10/09/16 Pct Recovery = 94% Analysis Date = 09/29/16 Pct Recovery = 93% Analysis Date = 09/29/16 Pct Recovery = 93% Analysis Date = 09/20/16 Pct Recovery = 93% Analysis Date = 09/20/16 Pct Recovery = 93% Analysis Date = 09/10/16 Pct Recovery = 93% Analysis Date = 09/10/16 Pct Recovery = 93% Analysis Date = 09/01/16 Pct Recovery = 93% Analysis Date = 09/01/16 Pct Recovery = 93% Analysis Date = 08/23/16 Pct Recovery = 93% Analysis Date = 08/23/16 Pct Recovery = 93% Analysis Date = 08/13/16 Pct Recovery = 93% Analysis Date = 08/13/16 Pct Recovery = 93% Analysis Date = 08/04/16 Pct Recovery = 93% Analysis Date = 08/04/16 Pct Recovery = 93% Analysis Date = 07/25/16 Pct Recovery = 93% Analysis Date = 07/25/16 Pct Recovery = 93% Analysis Date = 07/16/16 Pct Recovery = 93% Analysis Date = 07/16/16 Pct Recovery = 93% Analysis Date = 07/07/16 Pct Recovery = 93% Analysis Date = 07/07/16 Pct Recovery = 93% Analysis Date = 06/27/16 Pct Recovery = 93% Analysis Date = 06/27/16 Pct Recovery = 93% Analysis Date = 06/18/16 Pct Recovery = 93% Analysis Date = 06/18/16 Pct Recovery = 93% Analysis Date = 06/08/16 Pct Recovery = 93% Analysis Date = 06/08/16 Pct Recovery = 93% Analysis Date = 05/30/16 Pct Recovery = 93% Analysis Date = 05/30/16 Pct Recovery = 93% Analysis Date = 05/21/16 Pct Recovery = 93% Analysis Date = 05/21/16 Pct Recovery = 93% Analysis Date = 05/11/16 Pct Recovery = 93% Analysis Date = 05/11/16 Pct Recovery = 93% Analysis Date = 05/02/16 Pct Recovery = 93% Analysis Date = 05/02/16 Pct Recovery = 93% Analysis Date = 04/22/16 Pct Recovery = 93% Analysis Date = 04/22/16 Pct Recovery = 93% Analysis Date = 04/13/16 Pct Recovery = 93% Analysis Date = 04/13/16 Pct Recovery = 93% Analysis Date = 04/04/16 Pct Recovery = 93% Analysis Date = 04/04/16 Pct Recovery = 93% Analysis Date = 03/25/16 Pct Recovery = 93% Analysis Date = 03/25/16 Pct Recovery = 93% Analysis Date = 03/16/16 Pct Recovery = 93% Analysis Date = 03/16/16 Pct Recovery = 93% Analysis Date = 03/06/16 Pct Recovery = 93% Analysis Date = 03/06/16 Pct Recovery = 93% Analysis Date = 02/26/16 Pct Recovery = 92% Analysis Date = 02/26/16 Pct Recovery = 92% Analysis Date = 02/17/16 Pct Recovery = 92% Analysis Date = 02/17/16 Pct Recovery = 92% Analysis Date = 02/07/16 Pct Recovery = 92% Analysis Date = 02/07/16 Pct Recovery = 92% Analysis Date = 01/29/16 Pct Recovery = 92% Analysis Date = 01/29/16 Pct Recovery = 92% Analysis Date = 01/19/16 Pct Recovery = 92% Analysis Date = 01/19/16 Pct Recovery = 92% Analysis Date = 01/10/16 Pct Recovery = 92% Analysis Date = 01/10/16 Pct Recovery = 92% Analysis Date = 01/01/16 Pct Recovery = 92% Analysis Date = 01/01/16 Pct Recovery = 92% Analysis Date = 12/22/15 Pct Recovery = 92% Analysis Date = 12/22/15 Pct Recovery = 92% Analysis Date = 12/13/15 Pct Recovery = 92% Analysis Date = 12/13/15 Pct Recovery = 92% Analysis Date = 12/03/15 Pct Recovery = 92% Analysis Date = 12/03/15 Pct Recovery = 92% Analysis Date = 11/24/15 Pct Recovery = 92% Analysis Date = 11/24/15 Pct Recovery = 92% Analysis Date = 11/15/15 Pct Recovery = 92% Analysis Date = 11/15/15 Pct Recovery = 92% Analysis Date = 11/05/15 Pct Recovery = 92% Analysis Date = 11/05/15 Pct Recovery = 92% Analysis Date = 10/27/15 Pct Recovery = 92% Analysis Date = 10/27/15 Pct Recovery = 92% Analysis Date = 10/17/15 Pct Recovery = 92% Analysis Date = 10/17/15 Pct Recovery = 92% Analysis Date = 10/08/15 Pct Recovery = 92% Analysis Date = 10/08/15 Pct Recovery = 92% Analysis Date = 09/29/15 Pct Recovery = 92% Analysis Date = 09/29/15 Pct Recovery = 92% Analysis Date = 09/19/15 Pct Recovery = 92% Analysis Date = 09/19/15 Pct Recovery = 92% Analysis Date = 09/10/15 Pct Recovery = 92% Analysis Date = 09/10/15 Pct Recovery = 92% Analysis Date = 08/31/15 Pct Recovery = 91% Analysis Date = 08/31/15 Pct Recovery = 91% Analysis Date = 08/22/15 Pct Recovery = 91% Analysis Date = 08/22/15 Pct Recovery = 91% Analysis Date = 08/13/15 Pct Recovery = 91% Analysis Date = 08/13/15 Pct Recovery = 91% Analysis Date = 08/03/15 Pct Recovery = 91% Analysis Date = 08/03/15 Pct Recovery = 91% Analysis Date = 07/25/15 Pct Recovery = 91% Analysis Date = 07/25/15 Pct Recovery = 91% Analysis Date = 07/15/15 Pct Recovery = 91% Analysis Date = 07/15/15 Pct Recovery = 91% Analysis Date = 07/06/15 Pct Recovery = 91% Analysis Date = 07/06/15 Pct Recovery = 91% Analysis Date = 06/27/15 Pct Recovery = 91% Analysis Date = 06/27/15 Pct Recovery = 91% Analysis Date = 06/17/15 Pct Recovery = 91% Analysis Date = 06/17/15 Pct Recovery = 91% Analysis Date = 06/08/15 Pct Recovery = 91% Analysis Date = 06/08/15 Pct Recovery = 91% Analysis Date = 05/29/15 Pct Recovery = 91% Analysis Date = 05/29/15 Pct Recovery = 91% Analysis Date = 05/20/15 Pct Recovery = 91% Analysis Date = 05/20/15 Pct Recovery = 91% Analysis Date = 05/11/15 Pct Recovery = 91% Analysis Date = 05/11/15 Pct Recovery = 91% Analysis Date = 05/01/15 Pct Recovery = 91% Analysis Date = 05/01/15 Pct Recovery = 91% Analysis Date = 04/22/15 Pct Recovery = 92% Analysis Date = 04/22/15 Pct Recovery = 92% Analysis Date = 04/12/15 Pct Recovery = 92% Analysis Date = 04/12/15 Pct Recovery = 92% Analysis Date = 04/03/15 Pct Recovery = 92% Analysis Date = 04/03/15 Pct Recovery = 92% Analysis Date = 03/25/15 Pct Recovery = 92% Analysis Date = 03/25/15 Pct Recovery = 92% Analysis Date = 03/15/15 Pct Recovery = 92% Analysis Date = 03/15/15 Pct Recovery = 92% Analysis Date = 03/06/15 Pct Recovery = 92% Analysis Date = 03/06/15 Pct Recovery = 92% Analysis Date = 02/24/15 Pct Recovery = 92% Analysis Date = 02/24/15 Pct Recovery = 92% Analysis Date = 02/15/15 Pct Recovery = 92% Analysis Date = 02/15/15 Pct Recovery = 92% Analysis Date = 02/06/15 Pct Recovery = 92% Analysis Date = 02/06/15 Pct Recovery = 92% Analysis Date = 01/27/15 Pct Recovery = 92% Analysis Date = 01/27/15 Pct Recovery = 92% Analysis Date = 01/18/15 Pct Recovery = 92% Analysis Date = 01/18/15 Pct Recovery = 92% Analysis Date = 01/08/15 Pct Recovery = 92% Analysis Date = 01/08/15 Pct Recovery = 92% Analysis Date = 12/30/14 Pct Recovery = 92% Analysis Date = 12/30/14 Pct Recovery = 92% Analysis Date = 12/21/14 Pct Recovery = 92% Analysis Date = 12/21/14 Pct Recovery = 92% Analysis Date = 12/11/14 Pct Recovery = 92% Analysis Date = 12/11/14 Pct Recovery = 92% Analysis Date = 12/02/14 Pct Recovery = 92% Analysis Date = 12/02/14 Pct Recovery = 92% Analysis Date = 11/22/14 Pct Recovery = 92% Analysis Date = 11/22/14 Pct Recovery = 92% Analysis Date = 11/13/14 Pct Recovery = 92% Analysis Date = 11/13/14 Pct Recovery = 92% Analysis Date = 11/04/14 Pct Recovery = 92% Analysis Date = 11/04/14 Pct Recovery = 92% Analysis Date = 10/25/14 Pct Recovery = 92% Analysis Date = 10/25/14 Pct Recovery = 92% Analysis Date = 10/16/14 Pct Recovery = 92% Analysis Date = 10/16/14 Pct Recovery = 92% Analysis Date = 10/06/14 Pct Recovery = 92% Analysis Date = 10/06/14 Pct Recovery = 92% Analysis Date = 09/27/14 Pct Recovery = 92% Analysis Date = 09/27/14 Pct Recovery = 92% Analysis Date = 09/18/14 Pct Recovery = 92% Analysis Date = 09/18/14 Pct Recovery = 92% Analysis Date = 09/08/14 Pct Recovery = 91% Analysis Date = 09/08/14 Pct Recovery = 91% Analysis Date = 08/30/14 Pct Recovery = 91% Analysis Date = 08/30/14 Pct Recovery = 91% Analysis Date = 08/20/14 Pct Recovery = 91% Analysis Date = 08/20/14 Pct Recovery = 91% Analysis Date = 08/11/14 Pct Recovery = 91% Analysis Date = 08/11/14 Pct Recovery = 91% Analysis Date = 08/02/14 Pct Recovery = 91% Analysis Date = 08/02/14 Pct Recovery = 91% Analysis Date = 07/23/14 Pct Recovery = 91% Analysis Date = 07/23/14 Pct Recovery = 91% Analysis Date = 07/14/14 Pct Recovery = 91% Analysis Date = 07/14/14 Pct Recovery = 91% Analysis Date = 07/04/14 Pct Recovery = 91% Analysis Date = 07/04/14 Pct Recovery = 91% Analysis Date = 06/25/14 Pct Recovery = 91% Analysis Date = 06/25/14 Pct Recovery = 91% Analysis Date = 06/16/14 Pct Recovery = 90% Analysis Date = 06/16/14 Pct Recovery = 90% Analysis Date = 06/06/14 Pct Recovery = 90% Analysis Date = 06/06/14 Pct Recovery = 90% Analysis Date = 05/28/14 Pct Recovery = 90% Analysis Date = 05/28/14 Pct Recovery = 90% Analysis Date = 05/18/14 Pct Recovery = 90% Analysis Date = 05/18/14 Pct Recovery = 90% Analysis Date = 05/09/14 Pct Recovery = 90% Analysis Date = 05/09/14 Pct Recovery = 90% Analysis Date = 04/30/14 Pct Recovery = 90% Analysis Date = 04/30/14 Pct Recovery = 90% Analysis Date = 04/20/14 Pct Recovery = 90% Analysis Date = 04/20/14 Pct Recovery = 90% Analysis Date = 04/11/14 Pct Recovery = 90% Analysis Date = 04/11/14 Pct Recovery = 90% Analysis Date = 04/01/14 Pct Recovery = 90% Analysis Date = 04/01/14 Pct Recovery = 90% Analysis Date = 03/23/14 Pct Recovery = 90% Analysis Date = 03/23/14 Pct Recovery = 90% Analysis Date = 03/14/14 Pct Recovery = 90% Analysis Date = 03/14/14 Pct Recovery = 90% Analysis Date = 03/04/14 Pct Recovery = 90% Analysis Date = 03/04/14 Pct Recovery = 90% Analysis Date = 02/23/14 Pct Recovery = 89% Analysis Date = 02/23/14 Pct Recovery = 89% Analysis Date = 02/13/14 Pct Recovery = 89% Analysis Date = 02/13/14 Pct Recovery = 89% Analysis Date = 02/04/14 Pct Recovery = 89% Analysis Date = 02/04/14 Pct Recovery = 89% Analysis Date = 01/26/14 Pct Recovery = 89% Analysis Date = 01/26/14 Pct Recovery = 89% Analysis Date = 01/16/14 Pct Recovery = 89% Analysis Date = 01/16/14 Pct Recovery = 89% Analysis Date = 01/07/14 Pct Recovery = 89% Analysis Date = 01/07/14 Pct Recovery = 89% Analysis Date = 12/28/13 Pct Recovery = 89% Analysis Date = 12/28/13 Pct Recovery = 89% Analysis Date = 12/19/13 Pct Recovery = 89% Analysis Date = 12/19/13 Pct Recovery = 89% Analysis Date = 12/10/13 Pct Recovery = 89% Analysis Date = 12/10/13 Pct Recovery = 89% Analysis Date = 11/30/13 Pct Recovery = 89% Analysis Date = 11/30/13 Pct Recovery = 89% Analysis Date = 11/21/13 Pct Recovery = 89% Analysis Date = 11/21/13 Pct Recovery = 89% Analysis Date = 11/11/13 Pct Recovery = 89% Analysis Date = 11/11/13 Pct Recovery = 89% Analysis Date = 11/02/13 Pct Recovery = 89% Analysis Date = 11/02/13 Pct Recovery = 89% Analysis Date = 10/24/13 Pct Recovery = 88% Analysis Date = 10/24/13 Pct Recovery = 88% Analysis Date = 10/14/13 Pct Recovery = 88% Analysis Date = 10/14/13 Pct Recovery = 88% Analysis Date = 10/05/13 Pct Recovery = 88% Analysis Date = 10/05/13 Pct Recovery = 88% Analysis Date = 09/25/13 Pct Recovery = 88% Analysis Date = 09/25/13 Pct Recovery = 88% Analysis Date = 09/16/13 Pct Recovery = 88% Analysis Date = 09/16/13 Pct Recovery = 88% Analysis Date = 09/07/13 Pct Recovery = 88% Analysis Date = 09/07/13 Pct Recovery = 88% Analysis Date = 08/28/13 Pct Recovery = 88% Analysis Date = 08/28/13 Pct Recovery = 88% Analysis Date = 08/19/13 Pct Recovery = 88% Analysis Date = 08/19/13 Pct Recovery = 88% Analysis Date = 08/09/13 Pct Recovery = 88% Analysis Date = 08/09/13 Pct Recovery = 88% Analysis Date = 07/31/13 Pct Recovery = 88% Analysis Date = 07/31/13 Pct Recovery = 88% Analysis Date = 07/22/13 Pct Recovery = 88% Analysis Date = 07/22/13 Pct Recovery = 88% Analysis Date = 07/12/13 Pct Recovery = 88% Analysis Date = 07/12/13 Pct Recovery = 88% Analysis Date = 07/03/13 Pct Recovery = 88% Analysis Date = 07/03/13 Pct Recovery = 88% Analysis Date = 06/23/13 Pct Recovery = 88% Analysis Date = 06/23/13 Pct Recovery = 88% Analysis Date = 06/14/13 Pct Recovery = 88% Analysis Date = 06/14/13 Pct Recovery = 88% Analysis Date = 06/05/13 Pct Recovery = 88% Analysis Date = 06/05/13 Pct Recovery = 88% Analysis Date = 05/26/13 Pct Recovery = 87% Analysis Date = 05/26/13 Pct Recovery = 87% Analysis Date = 05/17/13 Pct Recovery = 87% Analysis Date = 05/17/13 Pct Recovery = 87% Analysis Date = 05/07/13 Pct Recovery = 87% Analysis Date = 05/07/13 Pct Recovery = 87% Analysis Date = 04/28/13 Pct Recovery = 87% Analysis Date = 04/28/13 Pct Recovery = 87% Analysis Date = 04/19/13 Pct Recovery = 87% Analysis Date = 04/19/13 Pct Recovery = 87% Analysis Date = 04/09/13 Pct Recovery = 87% Analysis Date = 04/09/13 Pct Recovery = 87% Analysis Date = 03/31/13 Pct Recovery = 87% Analysis Date = 03/31/13 Pct Recovery = 87% Analysis Date = 03/21/13 Pct Recovery = 87% Analysis Date = 03/21/13 Pct Recovery = 87% Analysis Date = 03/12/13 Pct Recovery = 87% Analysis Date = 03/12/13 Pct Recovery = 87% Analysis Date = 03/03/13 Pct Recovery = 87% Analysis Date = 03/03/13 Pct Recovery = 87% Analysis Date = 02/21/13 Pct Recovery = 87% Analysis Date = 02/21/13 Pct Recovery = 87% Analysis Date = 02/12/13 Pct Recovery = 87% Analysis Date = 02/12/13 Pct Recovery = 87% Analysis Date = 02/02/13 Pct Recovery = 87% Analysis Date = 02/02/13 Pct Recovery = 87% Analysis Date = 01/24/13 Pct Recovery = 87% Analysis Date = 01/24/13 Pct Recovery = 87% Analysis Date = 01/15/13 Pct Recovery = 87% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
METALAXYL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 73 92% 17% 90% 16%
Total 73 92% 17% 90% 16%

Sample Statistics
METALAXYL

Characteristic N % % Basis
Plotted 73 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 73 .  
False Negatives 0 0% 0 out of 73
Not Spiked 45 .  
False Positives 0 0% 0 out of 45

OBSP Determination:
METHIDATHION (SUPRACIDE)
METHOD: 2033 , TESTIDCODE: 61598GCM39

Laboratory ID = 20132490342 Lab Value = 0.098 Expected Conc. = 0.119 Report level label = 0.012 Pct Recovery = 83% Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20172510330 Lab Value = 0.067 Expected Conc. = 0.08 Report level label = 0.012 Pct Recovery = 84% Analysis Date = 12/29/17 SpikeMix = ChemService 6537100: 100 µl & Abs 071817Pest: 100 µl SpecificMix = 6537100 Laboratory ID = 20130940097 Lab Value = 0.054 Expected Conc. = 0.076 Report level label = 0.012 Pct Recovery = 71% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = 0507-12-04.2 Laboratory ID = 20123560092 Lab Value = 0.057 Expected Conc. = 0.076 Report level label = 0.012 Pct Recovery = 74% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = 0507-12-04.2 Laboratory ID = 20161880109 Lab Value = 0.073 Expected Conc. = 0.075 Report level label = 0.012 Pct Recovery = 97% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl SpecificMix = 03FF076 Laboratory ID = 20130810108 Lab Value = 0.064 Expected Conc. = 0.075 Report level label = 0.012 Pct Recovery = 85% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl SpecificMix = LB92783 Laboratory ID = 20130100066 Lab Value = 0.060 Expected Conc. = 0.075 Report level label = 0.012 Pct Recovery = 80% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl SpecificMix = LB92783 Laboratory ID = 20163370001 Lab Value = 0.074 Expected Conc. = 0.0746 Report level label = 0.012 Pct Recovery = 99% Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl SpecificMix = B20160331 Laboratory ID = 20163150006 Lab Value = 0.057 Expected Conc. = 0.0746 Report level label = 0.012 Pct Recovery = 76% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl SpecificMix = B20160331 Laboratory ID = 20152610011 Lab Value = 0.055 Expected Conc. = 0.0724 Report level label = 0.012 Pct Recovery = 76% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl SpecificMix = 0406-15-01 Laboratory ID = 20152460215 Lab Value = 0.047 Expected Conc. = 0.0724 Report level label = 0.012 Pct Recovery = 65% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl SpecificMix = 0406-15-01 Laboratory ID = 20172020035 Lab Value = 0.068 Expected Conc. = 0.062 Report level label = 0.012 Pct Recovery = 110% Analysis Date = 11/07/17 SpikeMix = Abs 071717Pest: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20170960001 Lab Value = 0.051 Expected Conc. = 0.06 Report level label = 0.012 Pct Recovery = 84% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl SpecificMix = 03FF076 Laboratory ID = 20132140002 Lab Value = 0.051 Expected Conc. = 0.06 Report level label = 0.012 Pct Recovery = 85% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl SpecificMix = LB99392 Laboratory ID = 20131370001 Lab Value = 0.069 Expected Conc. = 0.06 Report level label = 0.012 Pct Recovery = 116% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl SpecificMix = LB99392 Laboratory ID = 20171720140 Lab Value = 0.063 Expected Conc. = 0.0597 Report level label = 0.012 Pct Recovery = 105% Analysis Date = 08/31/17 SpikeMix = Supelco LC20138V: 80 µl & Phenova B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20171660002 Lab Value = 0.058 Expected Conc. = 0.0597 Report level label = 0.012 Pct Recovery = 98% Analysis Date = 08/23/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20170190026 Lab Value = 0.050 Expected Conc. = 0.0597 Report level label = 0.012 Pct Recovery = 84% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20161470001 Lab Value = 0.046 Expected Conc. = 0.0597 Report level label = 0.012 Pct Recovery = 78% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20140370077 Lab Value = 0.046 Expected Conc. = 0.0595 Report level label = 0.012 Pct Recovery = 77% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20132560001 Lab Value = 0.045 Expected Conc. = 0.0595 Report level label = 0.012 Pct Recovery = 76% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20150430092 Lab Value = 0.045 Expected Conc. = 0.0481 Report level label = 0.012 Pct Recovery = 94% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl SpecificMix = E1140407002 Laboratory ID = 20143110108 Lab Value = 0.045 Expected Conc. = 0.0481 Report level label = 0.012 Pct Recovery = 94% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl SpecificMix = E1140407002 Laboratory ID = 20142720002 Lab Value = 0.045 Expected Conc. = 0.0481 Report level label = 0.012 Pct Recovery = 93% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl SpecificMix = E1140407002 Laboratory ID = 20141770149 Lab Value = 0.041 Expected Conc. = 0.0481 Report level label = 0.012 Pct Recovery = 85% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl SpecificMix = E1140407002 Laboratory ID = 20143240095 Lab Value = 0.051 Expected Conc. = 0.048 Report level label = 0.012 Pct Recovery = 105% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl SpecificMix = 032714 Laboratory ID = 20142270001 Lab Value = 0.043 Expected Conc. = 0.048 Report level label = 0.012 Pct Recovery = 90% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl SpecificMix = 032714 Laboratory ID = 20141220025 Lab Value = 0.050 Expected Conc. = 0.048 Report level label = 0.012 Pct Recovery = 104% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl SpecificMix = 032714 Laboratory ID = 20172370001 Lab Value = 0.048 Expected Conc. = 0.04 Report level label = 0.012 Pct Recovery = 119% Analysis Date = 11/18/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6537100: 50 µl SpecificMix = 6537100 Laboratory ID = 20172230001 Lab Value = 0.049 Expected Conc. = 0.04 Report level label = 0.012 Pct Recovery = 123% Analysis Date = 10/19/17 SpikeMix = ChemService 6472100: 50 µl & Abs 071717Pest: 50 µl SpecificMix = 071717Pest Laboratory ID = 20160770090 Lab Value = 0.029 Expected Conc. = 0.0362 Report level label = 0.012 Pct Recovery = 80% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20160630046 Lab Value = 0.021 Expected Conc. = 0.0362 Report level label = 0.012 Pct Recovery = 59% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20153510109 Lab Value = 0.025 Expected Conc. = 0.0362 Report level label = 0.012 Pct Recovery = 70% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20153440001 Lab Value = 0.026 Expected Conc. = 0.0362 Report level label = 0.012 Pct Recovery = 72% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20161260151 Lab Value = 0.034 Expected Conc. = 0.036 Report level label = 0.012 Pct Recovery = 95% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = 3851600 Laboratory ID = 20151550293 Lab Value = 0.036 Expected Conc. = 0.036 Report level label = 0.012 Pct Recovery = 101% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl SpecificMix = 3851600 Laboratory ID = 20151270112 Lab Value = 0.037 Expected Conc. = 0.036 Report level label = 0.012 Pct Recovery = 102% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl SpecificMix = 3851600 Laboratory ID = 20130510051 Lab Value = 0.026 Expected Conc. = 0.0304 Report level label = 0.012 Pct Recovery = 84% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl SpecificMix = 0507-12-04.2 Laboratory ID = 20171510080 Lab Value = 0.033 Expected Conc. = 0.03 Report level label = 0.012 Pct Recovery = 109% Analysis Date = 06/09/17 SpikeMix = Supelco LC20138V: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20170460061 Lab Value = 0.027 Expected Conc. = 0.03 Report level label = 0.012 Pct Recovery = 89% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl SpecificMix = 03FF076 Laboratory ID = 20162660005 Lab Value = 0.032 Expected Conc. = 0.03 Report level label = 0.012 Pct Recovery = 105% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl SpecificMix = 03FF076 Laboratory ID = 20161600087 Lab Value = 0.026 Expected Conc. = 0.03 Report level label = 0.012 Pct Recovery = 86% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20161340228 Lab Value = 0.028 Expected Conc. = 0.03 Report level label = 0.012 Pct Recovery = 92% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl SpecificMix = 03FF076 Laboratory ID = 20161190075 Lab Value = 0.029 Expected Conc. = 0.03 Report level label = 0.012 Pct Recovery = 95% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20130390105 Lab Value = 0.024 Expected Conc. = 0.03 Report level label = 0.012 Pct Recovery = 81% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl SpecificMix = LB92783 Laboratory ID = 20171160110 Lab Value = 0.029 Expected Conc. = 0.0298 Report level label = 0.012 Pct Recovery = 96% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = B20160331 Laboratory ID = 20162380004 Lab Value = 0.026 Expected Conc. = 0.0298 Report level label = 0.012 Pct Recovery = 88% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = B20160331 Laboratory ID = 20162150213 Lab Value = 0.037 Expected Conc. = 0.0298 Report level label = 0.012 Pct Recovery = 125% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl SpecificMix = B20160331 Laboratory ID = 20142470041 Lab Value = 0.023 Expected Conc. = 0.0241 Report level label = 0.012 Pct Recovery = 94% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141910243 Lab Value = 0.020 Expected Conc. = 0.0241 Report level label = 0.012 Pct Recovery = 85% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141640076 Lab Value = 0.021 Expected Conc. = 0.0241 Report level label = 0.012 Pct Recovery = 87% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141360094 Lab Value = 0.020 Expected Conc. = 0.0241 Report level label = 0.012 Pct Recovery = 83% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = E1140407002 Laboratory ID = 20173120093 Lab Value = 0.024 Expected Conc. = 0.024 Report level label = 0.012 Pct Recovery = 101% Analysis Date = 03/10/18 SpikeMix = ChemService 6472100: 30 µl & ChemService 6537100: 30 µl SpecificMix = 6537100 Laboratory ID = 20172780018 Lab Value = 0.028 Expected Conc. = 0.024 Report level label = 0.012 Pct Recovery = 115% Analysis Date = 02/08/18 SpikeMix = ChemService 6537100: 30 µl & Abs 071817Pest: 30 µl SpecificMix = 6537100 Laboratory ID = 20150150115 Lab Value = 0.033 Expected Conc. = 0.024 Report level label = 0.012 Pct Recovery = 136% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl SpecificMix = 032714 Laboratory ID = 20142820151 Lab Value = 0.024 Expected Conc. = 0.024 Report level label = 0.012 Pct Recovery = 98% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl SpecificMix = 032714 Laboratory ID = 20141490205 Lab Value = 0.022 Expected Conc. = 0.024 Report level label = 0.012 Pct Recovery = 90% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = 032714 Laboratory ID = 20141080004 Lab Value = 0.023 Expected Conc. = 0.024 Report level label = 0.012 Pct Recovery = 97% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl SpecificMix = 032714 Laboratory ID = 20140510043 Lab Value = 0.031 Expected Conc. = 0.024 Report level label = 0.012 Pct Recovery = 128% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl SpecificMix = LB99392 Laboratory ID = 20133470008 Lab Value = 0.021 Expected Conc. = 0.024 Report level label = 0.012 Pct Recovery = 89% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl SpecificMix = LB99392 Laboratory ID = 20133190012 Lab Value = 0.025 Expected Conc. = 0.024 Report level label = 0.012 Pct Recovery = 103% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = LB99392 Laboratory ID = 20133050050 Lab Value = 0.024 Expected Conc. = 0.024 Report level label = 0.012 Pct Recovery = 102% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl SpecificMix = LB99392 Laboratory ID = 20133580036 Lab Value = 0.016 Expected Conc. = 0.0238 Report level label = 0.012 Pct Recovery = 68% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20131790009 Lab Value = 0.017 Expected Conc. = 0.0238 Report level label = 0.012 Pct Recovery = 73% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20131510026 Lab Value = 0.027 Expected Conc. = 0.0238 Report level label = 0.012 Pct Recovery = 114% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20152190003 Lab Value = 0.015 Expected Conc. = 0.0181 Report level label = 0.012 Pct Recovery = 84% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = 0406-15-01 Laboratory ID = 20152040177 Lab Value = 0.023 Expected Conc. = 0.0181 Report level label = 0.012 Pct Recovery = 127% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl SpecificMix = 0406-15-01 Laboratory ID = 20160430111 Lab Value = 0.013 Expected Conc. = 0.018 Report level label = 0.012 Pct Recovery = 72% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 3851600 Laboratory ID = 20160210080 Lab Value = 0.010 Expected Conc. = 0.018 Report level label = 0.012 Pct Recovery = 57% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 3851600 Laboratory ID = 20152950078 Lab Value = 0.014 Expected Conc. = 0.018 Report level label = 0.012 Pct Recovery = 77% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 3851600 Laboratory ID = 20153030068 Lab Value = 0.017 Expected Conc. = 0.018 Report level label = 0.012 Pct Recovery = 96% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = 3851600 Laboratory ID = 20151760208 Lab Value = 0.034 Expected Conc. = 0.018 Report level label = 0.012 Pct Recovery = 190% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl SpecificMix = 3851600 Laboratory ID = 20151380009 Lab Value = 0.018 Expected Conc. = 0.018 Report level label = 0.012 Pct Recovery = 98% Analysis Date = 05/30/15 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 3851600 Analysis Date = 03/10/18 Pct Recovery = 108% Analysis Date = 02/28/18 Pct Recovery = 107% Analysis Date = 02/28/18 Pct Recovery = 107% Analysis Date = 02/19/18 Pct Recovery = 107% Analysis Date = 02/19/18 Pct Recovery = 107% Analysis Date = 02/09/18 Pct Recovery = 107% Analysis Date = 02/09/18 Pct Recovery = 107% Analysis Date = 01/31/18 Pct Recovery = 106% Analysis Date = 01/31/18 Pct Recovery = 106% Analysis Date = 01/22/18 Pct Recovery = 106% Analysis Date = 01/22/18 Pct Recovery = 106% Analysis Date = 01/12/18 Pct Recovery = 106% Analysis Date = 01/12/18 Pct Recovery = 106% Analysis Date = 01/03/18 Pct Recovery = 105% Analysis Date = 01/03/18 Pct Recovery = 105% Analysis Date = 12/24/17 Pct Recovery = 105% Analysis Date = 12/24/17 Pct Recovery = 105% Analysis Date = 12/15/17 Pct Recovery = 105% Analysis Date = 12/15/17 Pct Recovery = 105% Analysis Date = 12/06/17 Pct Recovery = 104% Analysis Date = 12/06/17 Pct Recovery = 104% Analysis Date = 11/26/17 Pct Recovery = 104% Analysis Date = 11/26/17 Pct Recovery = 104% Analysis Date = 11/17/17 Pct Recovery = 104% Analysis Date = 11/17/17 Pct Recovery = 104% Analysis Date = 11/07/17 Pct Recovery = 104% Analysis Date = 11/07/17 Pct Recovery = 104% Analysis Date = 10/29/17 Pct Recovery = 103% Analysis Date = 10/29/17 Pct Recovery = 103% Analysis Date = 10/20/17 Pct Recovery = 103% Analysis Date = 10/20/17 Pct Recovery = 103% Analysis Date = 10/10/17 Pct Recovery = 103% Analysis Date = 10/10/17 Pct Recovery = 103% Analysis Date = 10/01/17 Pct Recovery = 102% Analysis Date = 10/01/17 Pct Recovery = 102% Analysis Date = 09/21/17 Pct Recovery = 102% Analysis Date = 09/21/17 Pct Recovery = 102% Analysis Date = 09/12/17 Pct Recovery = 102% Analysis Date = 09/12/17 Pct Recovery = 102% Analysis Date = 09/03/17 Pct Recovery = 101% Analysis Date = 09/03/17 Pct Recovery = 101% Analysis Date = 08/24/17 Pct Recovery = 101% Analysis Date = 08/24/17 Pct Recovery = 101% Analysis Date = 08/15/17 Pct Recovery = 101% Analysis Date = 08/15/17 Pct Recovery = 101% Analysis Date = 08/05/17 Pct Recovery = 100% Analysis Date = 08/05/17 Pct Recovery = 100% Analysis Date = 07/27/17 Pct Recovery = 100% Analysis Date = 07/27/17 Pct Recovery = 100% Analysis Date = 07/18/17 Pct Recovery = 100% Analysis Date = 07/18/17 Pct Recovery = 100% Analysis Date = 07/08/17 Pct Recovery = 100% Analysis Date = 07/08/17 Pct Recovery = 100% Analysis Date = 06/29/17 Pct Recovery = 99% Analysis Date = 06/29/17 Pct Recovery = 99% Analysis Date = 06/19/17 Pct Recovery = 99% Analysis Date = 06/19/17 Pct Recovery = 99% Analysis Date = 06/10/17 Pct Recovery = 99% Analysis Date = 06/10/17 Pct Recovery = 99% Analysis Date = 06/01/17 Pct Recovery = 98% Analysis Date = 06/01/17 Pct Recovery = 98% Analysis Date = 05/22/17 Pct Recovery = 98% Analysis Date = 05/22/17 Pct Recovery = 98% Analysis Date = 05/13/17 Pct Recovery = 98% Analysis Date = 05/13/17 Pct Recovery = 98% Analysis Date = 05/03/17 Pct Recovery = 97% Analysis Date = 05/03/17 Pct Recovery = 97% Analysis Date = 04/24/17 Pct Recovery = 97% Analysis Date = 04/24/17 Pct Recovery = 97% Analysis Date = 04/15/17 Pct Recovery = 97% Analysis Date = 04/15/17 Pct Recovery = 97% Analysis Date = 04/05/17 Pct Recovery = 97% Analysis Date = 04/05/17 Pct Recovery = 97% Analysis Date = 03/27/17 Pct Recovery = 96% Analysis Date = 03/27/17 Pct Recovery = 96% Analysis Date = 03/17/17 Pct Recovery = 96% Analysis Date = 03/17/17 Pct Recovery = 96% Analysis Date = 03/08/17 Pct Recovery = 96% Analysis Date = 03/08/17 Pct Recovery = 96% Analysis Date = 02/27/17 Pct Recovery = 95% Analysis Date = 02/27/17 Pct Recovery = 95% Analysis Date = 02/17/17 Pct Recovery = 95% Analysis Date = 02/17/17 Pct Recovery = 95% Analysis Date = 02/08/17 Pct Recovery = 95% Analysis Date = 02/08/17 Pct Recovery = 95% Analysis Date = 01/29/17 Pct Recovery = 95% Analysis Date = 01/29/17 Pct Recovery = 95% Analysis Date = 01/20/17 Pct Recovery = 94% Analysis Date = 01/20/17 Pct Recovery = 94% Analysis Date = 01/11/17 Pct Recovery = 94% Analysis Date = 01/11/17 Pct Recovery = 94% Analysis Date = 01/01/17 Pct Recovery = 94% Analysis Date = 01/01/17 Pct Recovery = 94% Analysis Date = 12/23/16 Pct Recovery = 94% Analysis Date = 12/23/16 Pct Recovery = 94% Analysis Date = 12/13/16 Pct Recovery = 93% Analysis Date = 12/13/16 Pct Recovery = 93% Analysis Date = 12/04/16 Pct Recovery = 93% Analysis Date = 12/04/16 Pct Recovery = 93% Analysis Date = 11/25/16 Pct Recovery = 93% Analysis Date = 11/25/16 Pct Recovery = 93% Analysis Date = 11/15/16 Pct Recovery = 92% Analysis Date = 11/15/16 Pct Recovery = 92% Analysis Date = 11/06/16 Pct Recovery = 92% Analysis Date = 11/06/16 Pct Recovery = 92% Analysis Date = 10/27/16 Pct Recovery = 92% Analysis Date = 10/27/16 Pct Recovery = 92% Analysis Date = 10/18/16 Pct Recovery = 92% Analysis Date = 10/18/16 Pct Recovery = 92% Analysis Date = 10/09/16 Pct Recovery = 91% Analysis Date = 10/09/16 Pct Recovery = 91% Analysis Date = 09/29/16 Pct Recovery = 91% Analysis Date = 09/29/16 Pct Recovery = 91% Analysis Date = 09/20/16 Pct Recovery = 91% Analysis Date = 09/20/16 Pct Recovery = 91% Analysis Date = 09/10/16 Pct Recovery = 91% Analysis Date = 09/10/16 Pct Recovery = 91% Analysis Date = 09/01/16 Pct Recovery = 90% Analysis Date = 09/01/16 Pct Recovery = 90% Analysis Date = 08/23/16 Pct Recovery = 90% Analysis Date = 08/23/16 Pct Recovery = 90% Analysis Date = 08/13/16 Pct Recovery = 90% Analysis Date = 08/13/16 Pct Recovery = 90% Analysis Date = 08/04/16 Pct Recovery = 90% Analysis Date = 08/04/16 Pct Recovery = 90% Analysis Date = 07/25/16 Pct Recovery = 90% Analysis Date = 07/25/16 Pct Recovery = 90% Analysis Date = 07/16/16 Pct Recovery = 90% Analysis Date = 07/16/16 Pct Recovery = 90% Analysis Date = 07/07/16 Pct Recovery = 90% Analysis Date = 07/07/16 Pct Recovery = 90% Analysis Date = 06/27/16 Pct Recovery = 90% Analysis Date = 06/27/16 Pct Recovery = 90% Analysis Date = 06/18/16 Pct Recovery = 89% Analysis Date = 06/18/16 Pct Recovery = 89% Analysis Date = 06/08/16 Pct Recovery = 89% Analysis Date = 06/08/16 Pct Recovery = 89% Analysis Date = 05/30/16 Pct Recovery = 89% Analysis Date = 05/30/16 Pct Recovery = 89% Analysis Date = 05/21/16 Pct Recovery = 89% Analysis Date = 05/21/16 Pct Recovery = 89% Analysis Date = 05/11/16 Pct Recovery = 89% Analysis Date = 05/11/16 Pct Recovery = 89% Analysis Date = 05/02/16 Pct Recovery = 90% Analysis Date = 05/02/16 Pct Recovery = 90% Analysis Date = 04/22/16 Pct Recovery = 90% Analysis Date = 04/22/16 Pct Recovery = 90% Analysis Date = 04/13/16 Pct Recovery = 90% Analysis Date = 04/13/16 Pct Recovery = 90% Analysis Date = 04/04/16 Pct Recovery = 90% Analysis Date = 04/04/16 Pct Recovery = 90% Analysis Date = 03/25/16 Pct Recovery = 90% Analysis Date = 03/25/16 Pct Recovery = 90% Analysis Date = 03/16/16 Pct Recovery = 91% Analysis Date = 03/16/16 Pct Recovery = 91% Analysis Date = 03/06/16 Pct Recovery = 91% Analysis Date = 03/06/16 Pct Recovery = 91% Analysis Date = 02/26/16 Pct Recovery = 91% Analysis Date = 02/26/16 Pct Recovery = 91% Analysis Date = 02/17/16 Pct Recovery = 91% Analysis Date = 02/17/16 Pct Recovery = 91% Analysis Date = 02/07/16 Pct Recovery = 91% Analysis Date = 02/07/16 Pct Recovery = 91% Analysis Date = 01/29/16 Pct Recovery = 91% Analysis Date = 01/29/16 Pct Recovery = 91% Analysis Date = 01/19/16 Pct Recovery = 92% Analysis Date = 01/19/16 Pct Recovery = 92% Analysis Date = 01/10/16 Pct Recovery = 92% Analysis Date = 01/10/16 Pct Recovery = 92% Analysis Date = 01/01/16 Pct Recovery = 92% Analysis Date = 01/01/16 Pct Recovery = 92% Analysis Date = 12/22/15 Pct Recovery = 92% Analysis Date = 12/22/15 Pct Recovery = 92% Analysis Date = 12/13/15 Pct Recovery = 92% Analysis Date = 12/13/15 Pct Recovery = 92% Analysis Date = 12/03/15 Pct Recovery = 92% Analysis Date = 12/03/15 Pct Recovery = 92% Analysis Date = 11/24/15 Pct Recovery = 92% Analysis Date = 11/24/15 Pct Recovery = 92% Analysis Date = 11/15/15 Pct Recovery = 92% Analysis Date = 11/15/15 Pct Recovery = 92% Analysis Date = 11/05/15 Pct Recovery = 93% Analysis Date = 11/05/15 Pct Recovery = 93% Analysis Date = 10/27/15 Pct Recovery = 93% Analysis Date = 10/27/15 Pct Recovery = 93% Analysis Date = 10/17/15 Pct Recovery = 93% Analysis Date = 10/17/15 Pct Recovery = 93% Analysis Date = 10/08/15 Pct Recovery = 93% Analysis Date = 10/08/15 Pct Recovery = 93% Analysis Date = 09/29/15 Pct Recovery = 93% Analysis Date = 09/29/15 Pct Recovery = 93% Analysis Date = 09/19/15 Pct Recovery = 93% Analysis Date = 09/19/15 Pct Recovery = 93% Analysis Date = 09/10/15 Pct Recovery = 93% Analysis Date = 09/10/15 Pct Recovery = 93% Analysis Date = 08/31/15 Pct Recovery = 94% Analysis Date = 08/31/15 Pct Recovery = 94% Analysis Date = 08/22/15 Pct Recovery = 94% Analysis Date = 08/22/15 Pct Recovery = 94% Analysis Date = 08/13/15 Pct Recovery = 94% Analysis Date = 08/13/15 Pct Recovery = 94% Analysis Date = 08/03/15 Pct Recovery = 94% Analysis Date = 08/03/15 Pct Recovery = 94% Analysis Date = 07/25/15 Pct Recovery = 94% Analysis Date = 07/25/15 Pct Recovery = 94% Analysis Date = 07/15/15 Pct Recovery = 94% Analysis Date = 07/15/15 Pct Recovery = 94% Analysis Date = 07/06/15 Pct Recovery = 94% Analysis Date = 07/06/15 Pct Recovery = 94% Analysis Date = 06/27/15 Pct Recovery = 95% Analysis Date = 06/27/15 Pct Recovery = 95% Analysis Date = 06/17/15 Pct Recovery = 95% Analysis Date = 06/17/15 Pct Recovery = 95% Analysis Date = 06/08/15 Pct Recovery = 95% Analysis Date = 06/08/15 Pct Recovery = 95% Analysis Date = 05/29/15 Pct Recovery = 95% Analysis Date = 05/29/15 Pct Recovery = 95% Analysis Date = 05/20/15 Pct Recovery = 95% Analysis Date = 05/20/15 Pct Recovery = 95% Analysis Date = 05/11/15 Pct Recovery = 96% Analysis Date = 05/11/15 Pct Recovery = 96% Analysis Date = 05/01/15 Pct Recovery = 96% Analysis Date = 05/01/15 Pct Recovery = 96% Analysis Date = 04/22/15 Pct Recovery = 96% Analysis Date = 04/22/15 Pct Recovery = 96% Analysis Date = 04/12/15 Pct Recovery = 96% Analysis Date = 04/12/15 Pct Recovery = 96% Analysis Date = 04/03/15 Pct Recovery = 96% Analysis Date = 04/03/15 Pct Recovery = 96% Analysis Date = 03/25/15 Pct Recovery = 96% Analysis Date = 03/25/15 Pct Recovery = 96% Analysis Date = 03/15/15 Pct Recovery = 97% Analysis Date = 03/15/15 Pct Recovery = 97% Analysis Date = 03/06/15 Pct Recovery = 97% Analysis Date = 03/06/15 Pct Recovery = 97% Analysis Date = 02/24/15 Pct Recovery = 97% Analysis Date = 02/24/15 Pct Recovery = 97% Analysis Date = 02/15/15 Pct Recovery = 97% Analysis Date = 02/15/15 Pct Recovery = 97% Analysis Date = 02/06/15 Pct Recovery = 97% Analysis Date = 02/06/15 Pct Recovery = 97% Analysis Date = 01/27/15 Pct Recovery = 97% Analysis Date = 01/27/15 Pct Recovery = 97% Analysis Date = 01/18/15 Pct Recovery = 97% Analysis Date = 01/18/15 Pct Recovery = 97% Analysis Date = 01/08/15 Pct Recovery = 97% Analysis Date = 01/08/15 Pct Recovery = 97% Analysis Date = 12/30/14 Pct Recovery = 97% Analysis Date = 12/30/14 Pct Recovery = 97% Analysis Date = 12/21/14 Pct Recovery = 97% Analysis Date = 12/21/14 Pct Recovery = 97% Analysis Date = 12/11/14 Pct Recovery = 98% Analysis Date = 12/11/14 Pct Recovery = 98% Analysis Date = 12/02/14 Pct Recovery = 98% Analysis Date = 12/02/14 Pct Recovery = 98% Analysis Date = 11/22/14 Pct Recovery = 98% Analysis Date = 11/22/14 Pct Recovery = 98% Analysis Date = 11/13/14 Pct Recovery = 98% Analysis Date = 11/13/14 Pct Recovery = 98% Analysis Date = 11/04/14 Pct Recovery = 98% Analysis Date = 11/04/14 Pct Recovery = 98% Analysis Date = 10/25/14 Pct Recovery = 98% Analysis Date = 10/25/14 Pct Recovery = 98% Analysis Date = 10/16/14 Pct Recovery = 98% Analysis Date = 10/16/14 Pct Recovery = 98% Analysis Date = 10/06/14 Pct Recovery = 98% Analysis Date = 10/06/14 Pct Recovery = 98% Analysis Date = 09/27/14 Pct Recovery = 98% Analysis Date = 09/27/14 Pct Recovery = 98% Analysis Date = 09/18/14 Pct Recovery = 98% Analysis Date = 09/18/14 Pct Recovery = 98% Analysis Date = 09/08/14 Pct Recovery = 97% Analysis Date = 09/08/14 Pct Recovery = 97% Analysis Date = 08/30/14 Pct Recovery = 97% Analysis Date = 08/30/14 Pct Recovery = 97% Analysis Date = 08/20/14 Pct Recovery = 97% Analysis Date = 08/20/14 Pct Recovery = 97% Analysis Date = 08/11/14 Pct Recovery = 97% Analysis Date = 08/11/14 Pct Recovery = 97% Analysis Date = 08/02/14 Pct Recovery = 96% Analysis Date = 08/02/14 Pct Recovery = 96% Analysis Date = 07/23/14 Pct Recovery = 96% Analysis Date = 07/23/14 Pct Recovery = 96% Analysis Date = 07/14/14 Pct Recovery = 96% Analysis Date = 07/14/14 Pct Recovery = 96% Analysis Date = 07/04/14 Pct Recovery = 96% Analysis Date = 07/04/14 Pct Recovery = 96% Analysis Date = 06/25/14 Pct Recovery = 96% Analysis Date = 06/25/14 Pct Recovery = 96% Analysis Date = 06/16/14 Pct Recovery = 95% Analysis Date = 06/16/14 Pct Recovery = 95% Analysis Date = 06/06/14 Pct Recovery = 95% Analysis Date = 06/06/14 Pct Recovery = 95% Analysis Date = 05/28/14 Pct Recovery = 95% Analysis Date = 05/28/14 Pct Recovery = 95% Analysis Date = 05/18/14 Pct Recovery = 95% Analysis Date = 05/18/14 Pct Recovery = 95% Analysis Date = 05/09/14 Pct Recovery = 94% Analysis Date = 05/09/14 Pct Recovery = 94% Analysis Date = 04/30/14 Pct Recovery = 94% Analysis Date = 04/30/14 Pct Recovery = 94% Analysis Date = 04/20/14 Pct Recovery = 94% Analysis Date = 04/20/14 Pct Recovery = 94% Analysis Date = 04/11/14 Pct Recovery = 94% Analysis Date = 04/11/14 Pct Recovery = 94% Analysis Date = 04/01/14 Pct Recovery = 93% Analysis Date = 04/01/14 Pct Recovery = 93% Analysis Date = 03/23/14 Pct Recovery = 93% Analysis Date = 03/23/14 Pct Recovery = 93% Analysis Date = 03/14/14 Pct Recovery = 93% Analysis Date = 03/14/14 Pct Recovery = 93% Analysis Date = 03/04/14 Pct Recovery = 93% Analysis Date = 03/04/14 Pct Recovery = 93% Analysis Date = 02/23/14 Pct Recovery = 92% Analysis Date = 02/23/14 Pct Recovery = 92% Analysis Date = 02/13/14 Pct Recovery = 92% Analysis Date = 02/13/14 Pct Recovery = 92% Analysis Date = 02/04/14 Pct Recovery = 92% Analysis Date = 02/04/14 Pct Recovery = 92% Analysis Date = 01/26/14 Pct Recovery = 92% Analysis Date = 01/26/14 Pct Recovery = 92% Analysis Date = 01/16/14 Pct Recovery = 91% Analysis Date = 01/16/14 Pct Recovery = 91% Analysis Date = 01/07/14 Pct Recovery = 91% Analysis Date = 01/07/14 Pct Recovery = 91% Analysis Date = 12/28/13 Pct Recovery = 91% Analysis Date = 12/28/13 Pct Recovery = 91% Analysis Date = 12/19/13 Pct Recovery = 91% Analysis Date = 12/19/13 Pct Recovery = 91% Analysis Date = 12/10/13 Pct Recovery = 90% Analysis Date = 12/10/13 Pct Recovery = 90% Analysis Date = 11/30/13 Pct Recovery = 90% Analysis Date = 11/30/13 Pct Recovery = 90% Analysis Date = 11/21/13 Pct Recovery = 90% Analysis Date = 11/21/13 Pct Recovery = 90% Analysis Date = 11/11/13 Pct Recovery = 90% Analysis Date = 11/11/13 Pct Recovery = 90% Analysis Date = 11/02/13 Pct Recovery = 89% Analysis Date = 11/02/13 Pct Recovery = 89% Analysis Date = 10/24/13 Pct Recovery = 89% Analysis Date = 10/24/13 Pct Recovery = 89% Analysis Date = 10/14/13 Pct Recovery = 89% Analysis Date = 10/14/13 Pct Recovery = 89% Analysis Date = 10/05/13 Pct Recovery = 89% Analysis Date = 10/05/13 Pct Recovery = 89% Analysis Date = 09/25/13 Pct Recovery = 88% Analysis Date = 09/25/13 Pct Recovery = 88% Analysis Date = 09/16/13 Pct Recovery = 88% Analysis Date = 09/16/13 Pct Recovery = 88% Analysis Date = 09/07/13 Pct Recovery = 88% Analysis Date = 09/07/13 Pct Recovery = 88% Analysis Date = 08/28/13 Pct Recovery = 88% Analysis Date = 08/28/13 Pct Recovery = 88% Analysis Date = 08/19/13 Pct Recovery = 87% Analysis Date = 08/19/13 Pct Recovery = 87% Analysis Date = 08/09/13 Pct Recovery = 87% Analysis Date = 08/09/13 Pct Recovery = 87% Analysis Date = 07/31/13 Pct Recovery = 87% Analysis Date = 07/31/13 Pct Recovery = 87% Analysis Date = 07/22/13 Pct Recovery = 87% Analysis Date = 07/22/13 Pct Recovery = 87% Analysis Date = 07/12/13 Pct Recovery = 87% Analysis Date = 07/12/13 Pct Recovery = 87% Analysis Date = 07/03/13 Pct Recovery = 86% Analysis Date = 07/03/13 Pct Recovery = 86% Analysis Date = 06/23/13 Pct Recovery = 86% Analysis Date = 06/23/13 Pct Recovery = 86% Analysis Date = 06/14/13 Pct Recovery = 86% Analysis Date = 06/14/13 Pct Recovery = 86% Analysis Date = 06/05/13 Pct Recovery = 86% Analysis Date = 06/05/13 Pct Recovery = 86% Analysis Date = 05/26/13 Pct Recovery = 85% Analysis Date = 05/26/13 Pct Recovery = 85% Analysis Date = 05/17/13 Pct Recovery = 85% Analysis Date = 05/17/13 Pct Recovery = 85% Analysis Date = 05/07/13 Pct Recovery = 85% Analysis Date = 05/07/13 Pct Recovery = 85% Analysis Date = 04/28/13 Pct Recovery = 85% Analysis Date = 04/28/13 Pct Recovery = 85% Analysis Date = 04/19/13 Pct Recovery = 84% Analysis Date = 04/19/13 Pct Recovery = 84% Analysis Date = 04/09/13 Pct Recovery = 84% Analysis Date = 04/09/13 Pct Recovery = 84% Analysis Date = 03/31/13 Pct Recovery = 84% Analysis Date = 03/31/13 Pct Recovery = 84% Analysis Date = 03/21/13 Pct Recovery = 84% Analysis Date = 03/21/13 Pct Recovery = 84% Analysis Date = 03/12/13 Pct Recovery = 84% Analysis Date = 03/12/13 Pct Recovery = 84% Analysis Date = 03/03/13 Pct Recovery = 83% Analysis Date = 03/03/13 Pct Recovery = 83% Analysis Date = 02/21/13 Pct Recovery = 83% Analysis Date = 02/21/13 Pct Recovery = 83% Analysis Date = 02/12/13 Pct Recovery = 83% Analysis Date = 02/12/13 Pct Recovery = 83% Analysis Date = 02/02/13 Pct Recovery = 83% Analysis Date = 02/02/13 Pct Recovery = 83% Analysis Date = 01/24/13 Pct Recovery = 82% Analysis Date = 01/24/13 Pct Recovery = 82% Analysis Date = 01/15/13 Pct Recovery = 82% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
METHIDATHION (SUPRACIDE)

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 73 93% 20% 90% 16%
Total 73 93% 20% 90% 16%

Sample Statistics
METHIDATHION (SUPRACIDE)

Characteristic N % % Basis
Plotted 73 100% Spiked
Estimated Values 3 4% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 73 .  
False Negatives 0 0% 0 out of 73
Not Spiked 45 .  
False Positives 0 0% 0 out of 45

OBSP Determination:
METOLACHLOR
METHOD: 2033 , TESTIDCODE: 39415GCM35

Laboratory ID = 20132490342 Lab Value = 0.257 Expected Conc. = 0.256 Report level label = 0.012 Pct Recovery = 100% Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20130250061 Lab Value = 0.129 Expected Conc. = 0.149 Report level label = 0.012 Pct Recovery = 87% Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl SpecificMix = 05BB029 Laboratory ID = 20140370077 Lab Value = 0.119 Expected Conc. = 0.128 Report level label = 0.012 Pct Recovery = 93% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20132560001 Lab Value = 0.118 Expected Conc. = 0.128 Report level label = 0.012 Pct Recovery = 92% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20132140002 Lab Value = 0.115 Expected Conc. = 0.1252 Report level label = 0.012 Pct Recovery = 92% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl SpecificMix = LB99392 Laboratory ID = 20131370001 Lab Value = 0.145 Expected Conc. = 0.1252 Report level label = 0.012 Pct Recovery = 116% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl SpecificMix = LB99392 Laboratory ID = 20172510330 Lab Value = 0.077 Expected Conc. = 0.08 Report level label = 0.012 Pct Recovery = 96% Analysis Date = 12/29/17 SpikeMix = ChemService 6537100: 100 µl & Abs 071817Pest: 100 µl SpecificMix = 071817Pest Laboratory ID = 20163370001 Lab Value = 0.070 Expected Conc. = 0.0764 Report level label = 0.012 Pct Recovery = 91% Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl SpecificMix = B20160331 Laboratory ID = 20163150006 Lab Value = 0.065 Expected Conc. = 0.0764 Report level label = 0.012 Pct Recovery = 85% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl SpecificMix = B20160331 Laboratory ID = 20130940097 Lab Value = 0.052 Expected Conc. = 0.076 Report level label = 0.012 Pct Recovery = 69% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = 052412 Laboratory ID = 20130100066 Lab Value = 0.070 Expected Conc. = 0.076 Report level label = 0.012 Pct Recovery = 92% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl SpecificMix = 052412 Laboratory ID = 20140230082 Lab Value = 0.056 Expected Conc. = 0.0755 Report level label = 0.012 Pct Recovery = 74% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl SpecificMix = 012513 Laboratory ID = 20132420001 Lab Value = 0.054 Expected Conc. = 0.0755 Report level label = 0.012 Pct Recovery = 72% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl SpecificMix = 012513 Laboratory ID = 20161880109 Lab Value = 0.086 Expected Conc. = 0.074 Report level label = 0.012 Pct Recovery = 116% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl SpecificMix = 03FF076 Laboratory ID = 20152750006 Lab Value = 0.057 Expected Conc. = 0.0728 Report level label = 0.012 Pct Recovery = 78% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl SpecificMix = 040615 Laboratory ID = 20152610011 Lab Value = 0.059 Expected Conc. = 0.0728 Report level label = 0.012 Pct Recovery = 81% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl SpecificMix = 040615 Laboratory ID = 20171720140 Lab Value = 0.063 Expected Conc. = 0.0611 Report level label = 0.012 Pct Recovery = 102% Analysis Date = 08/31/17 SpikeMix = Supelco LC20138V: 80 µl & Phenova B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20171660002 Lab Value = 0.059 Expected Conc. = 0.0611 Report level label = 0.012 Pct Recovery = 96% Analysis Date = 08/23/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20170190026 Lab Value = 0.052 Expected Conc. = 0.0611 Report level label = 0.012 Pct Recovery = 85% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20161470001 Lab Value = 0.055 Expected Conc. = 0.0611 Report level label = 0.012 Pct Recovery = 89% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20170960001 Lab Value = 0.048 Expected Conc. = 0.0592 Report level label = 0.012 Pct Recovery = 81% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl SpecificMix = 03FF076 Laboratory ID = 20133580036 Lab Value = 0.035 Expected Conc. = 0.0512 Report level label = 0.012 Pct Recovery = 68% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20131790009 Lab Value = 0.034 Expected Conc. = 0.0512 Report level label = 0.012 Pct Recovery = 66% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20131510026 Lab Value = 0.036 Expected Conc. = 0.0512 Report level label = 0.012 Pct Recovery = 70% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20140510043 Lab Value = 0.034 Expected Conc. = 0.0501 Report level label = 0.012 Pct Recovery = 67% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl SpecificMix = LB99392 Laboratory ID = 20133470008 Lab Value = 0.047 Expected Conc. = 0.0501 Report level label = 0.012 Pct Recovery = 93% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl SpecificMix = LB99392 Laboratory ID = 20133190012 Lab Value = 0.049 Expected Conc. = 0.0501 Report level label = 0.012 Pct Recovery = 98% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = LB99392 Laboratory ID = 20133050050 Lab Value = 0.043 Expected Conc. = 0.0501 Report level label = 0.012 Pct Recovery = 86% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl SpecificMix = LB99392 Laboratory ID = 20150430092 Lab Value = 0.033 Expected Conc. = 0.048 Report level label = 0.012 Pct Recovery = 69% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl SpecificMix = E1140407002 Laboratory ID = 20143240095 Lab Value = 0.037 Expected Conc. = 0.048 Report level label = 0.012 Pct Recovery = 76% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl SpecificMix = 032714 Laboratory ID = 20143110108 Lab Value = 0.034 Expected Conc. = 0.048 Report level label = 0.012 Pct Recovery = 71% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl SpecificMix = E1140407002 Laboratory ID = 20142720002 Lab Value = 0.035 Expected Conc. = 0.048 Report level label = 0.012 Pct Recovery = 72% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl SpecificMix = E1140407002 Laboratory ID = 20142270001 Lab Value = 0.034 Expected Conc. = 0.048 Report level label = 0.012 Pct Recovery = 72% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl SpecificMix = 032714 Laboratory ID = 20141770149 Lab Value = 0.032 Expected Conc. = 0.048 Report level label = 0.012 Pct Recovery = 67% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl SpecificMix = E1140407002 Laboratory ID = 20141220025 Lab Value = 0.058 Expected Conc. = 0.048 Report level label = 0.012 Pct Recovery = 121% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl SpecificMix = 032714 Laboratory ID = 20172560101 Lab Value = 0.030 Expected Conc. = 0.04 Report level label = 0.012 Pct Recovery = 74% Analysis Date = 12/22/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6567600: 50 µl SpecificMix = 6567600 Laboratory ID = 20151900132 Lab Value = 0.027 Expected Conc. = 0.0364 Report level label = 0.012 Pct Recovery = 75% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl SpecificMix = 040615 Laboratory ID = 20151550293 Lab Value = 0.030 Expected Conc. = 0.0364 Report level label = 0.012 Pct Recovery = 82% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl SpecificMix = 040615 Laboratory ID = 20161260151 Lab Value = 0.027 Expected Conc. = 0.036 Report level label = 0.012 Pct Recovery = 76% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = EN150513008 Laboratory ID = 20160770090 Lab Value = 0.028 Expected Conc. = 0.036 Report level label = 0.012 Pct Recovery = 78% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = EN150513008 Laboratory ID = 20153510109 Lab Value = 0.027 Expected Conc. = 0.036 Report level label = 0.012 Pct Recovery = 74% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = EN150513008 Laboratory ID = 20152330039 Lab Value = 0.025 Expected Conc. = 0.036 Report level label = 0.012 Pct Recovery = 70% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl SpecificMix = EN150513008 Laboratory ID = 20171160110 Lab Value = 0.026 Expected Conc. = 0.0306 Report level label = 0.012 Pct Recovery = 85% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = B20160331 Laboratory ID = 20162380004 Lab Value = 0.026 Expected Conc. = 0.0306 Report level label = 0.012 Pct Recovery = 85% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = B20160331 Laboratory ID = 20162150213 Lab Value = 0.027 Expected Conc. = 0.0306 Report level label = 0.012 Pct Recovery = 88% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl SpecificMix = B20160331 Laboratory ID = 20133400002 Lab Value = 0.027 Expected Conc. = 0.0304 Report level label = 0.012 Pct Recovery = 89% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = 052412 Laboratory ID = 20132910008 Lab Value = 0.022 Expected Conc. = 0.0304 Report level label = 0.012 Pct Recovery = 73% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = 052412 Laboratory ID = 20130650005 Lab Value = 0.020 Expected Conc. = 0.0304 Report level label = 0.012 Pct Recovery = 67% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl SpecificMix = 052412 Laboratory ID = 20140860102 Lab Value = 0.021 Expected Conc. = 0.0302 Report level label = 0.012 Pct Recovery = 68% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 012513 Laboratory ID = 20131920149 Lab Value = 0.025 Expected Conc. = 0.0302 Report level label = 0.012 Pct Recovery = 84% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl SpecificMix = 012513 Laboratory ID = 20131230084 Lab Value = 0.033 Expected Conc. = 0.0298 Report level label = 0.012 Pct Recovery = 112% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl SpecificMix = 05BB029 Laboratory ID = 20130510051 Lab Value = 0.022 Expected Conc. = 0.0298 Report level label = 0.012 Pct Recovery = 74% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl SpecificMix = 05BB029 Laboratory ID = 20172020035 Lab Value = 0.032 Expected Conc. = 0.0296 Report level label = 0.012 Pct Recovery = 109% Analysis Date = 11/07/17 SpikeMix = Abs 071717Pest: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20171510080 Lab Value = 0.032 Expected Conc. = 0.0296 Report level label = 0.012 Pct Recovery = 108% Analysis Date = 06/09/17 SpikeMix = Supelco LC20138V: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20170460061 Lab Value = 0.023 Expected Conc. = 0.0296 Report level label = 0.012 Pct Recovery = 79% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl SpecificMix = 03FF076 Laboratory ID = 20162660005 Lab Value = 0.027 Expected Conc. = 0.0296 Report level label = 0.012 Pct Recovery = 92% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl SpecificMix = 03FF076 Laboratory ID = 20161600087 Lab Value = 0.027 Expected Conc. = 0.0296 Report level label = 0.012 Pct Recovery = 90% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20161340228 Lab Value = 0.024 Expected Conc. = 0.0296 Report level label = 0.012 Pct Recovery = 81% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl SpecificMix = 03FF076 Laboratory ID = 20161190075 Lab Value = 0.021 Expected Conc. = 0.0296 Report level label = 0.012 Pct Recovery = 72% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20172780018 Lab Value = 0.021 Expected Conc. = 0.024 Report level label = 0.012 Pct Recovery = 89% Analysis Date = 02/08/18 SpikeMix = ChemService 6537100: 30 µl & Abs 071817Pest: 30 µl SpecificMix = 071817Pest Laboratory ID = 20150150115 Lab Value = 0.018 Expected Conc. = 0.024 Report level label = 0.012 Pct Recovery = 77% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl SpecificMix = 032714 Laboratory ID = 20142820151 Lab Value = 0.019 Expected Conc. = 0.024 Report level label = 0.012 Pct Recovery = 81% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl SpecificMix = 032714 Laboratory ID = 20142470041 Lab Value = 0.021 Expected Conc. = 0.024 Report level label = 0.012 Pct Recovery = 88% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141910243 Lab Value = 0.017 Expected Conc. = 0.024 Report level label = 0.012 Pct Recovery = 73% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141640076 Lab Value = 0.021 Expected Conc. = 0.024 Report level label = 0.012 Pct Recovery = 86% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141490205 Lab Value = 0.023 Expected Conc. = 0.024 Report level label = 0.012 Pct Recovery = 94% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = 032714 Laboratory ID = 20141360094 Lab Value = 0.017 Expected Conc. = 0.024 Report level label = 0.012 Pct Recovery = 72% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141080004 Lab Value = 0.021 Expected Conc. = 0.024 Report level label = 0.012 Pct Recovery = 87% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl SpecificMix = 032714 Laboratory ID = 20161050143 Lab Value = 0.017 Expected Conc. = 0.0182 Report level label = 0.012 Pct Recovery = 91% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Laboratory ID = 20160430111 Lab Value = 0.017 Expected Conc. = 0.0182 Report level label = 0.012 Pct Recovery = 95% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Laboratory ID = 20160070059 Lab Value = 0.016 Expected Conc. = 0.0182 Report level label = 0.012 Pct Recovery = 88% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = 040615 Laboratory ID = 20151380009 Lab Value = 0.014 Expected Conc. = 0.0182 Report level label = 0.012 Pct Recovery = 75% Analysis Date = 05/30/15 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Laboratory ID = 20151210037 Lab Value = 0.017 Expected Conc. = 0.0182 Report level label = 0.012 Pct Recovery = 92% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Laboratory ID = 20160560044 Lab Value = 0.015 Expected Conc. = 0.018 Report level label = 0.012 Pct Recovery = 81% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl SpecificMix = EN150513008 Laboratory ID = 20153160001 Lab Value = 0.015 Expected Conc. = 0.018 Report level label = 0.012 Pct Recovery = 84% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = EN150513008 Laboratory ID = 20153030068 Lab Value = 0.016 Expected Conc. = 0.018 Report level label = 0.012 Pct Recovery = 86% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150513008 Laboratory ID = 20152190003 Lab Value = 0.013 Expected Conc. = 0.018 Report level label = 0.012 Pct Recovery = 73% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150513008 Laboratory ID = 20151480170 Lab Value = 0.015 Expected Conc. = 0.018 Report level label = 0.012 Pct Recovery = 81% Analysis Date = 06/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150513008 Analysis Date = 02/08/18 Pct Recovery = 95% Analysis Date = 01/29/18 Pct Recovery = 95% Analysis Date = 01/29/18 Pct Recovery = 95% Analysis Date = 01/20/18 Pct Recovery = 95% Analysis Date = 01/20/18 Pct Recovery = 95% Analysis Date = 01/11/18 Pct Recovery = 95% Analysis Date = 01/11/18 Pct Recovery = 95% Analysis Date = 01/02/18 Pct Recovery = 95% Analysis Date = 01/02/18 Pct Recovery = 95% Analysis Date = 12/23/17 Pct Recovery = 95% Analysis Date = 12/23/17 Pct Recovery = 95% Analysis Date = 12/14/17 Pct Recovery = 94% Analysis Date = 12/14/17 Pct Recovery = 94% Analysis Date = 12/05/17 Pct Recovery = 94% Analysis Date = 12/05/17 Pct Recovery = 94% Analysis Date = 11/26/17 Pct Recovery = 94% Analysis Date = 11/26/17 Pct Recovery = 94% Analysis Date = 11/16/17 Pct Recovery = 94% Analysis Date = 11/16/17 Pct Recovery = 94% Analysis Date = 11/07/17 Pct Recovery = 94% Analysis Date = 11/07/17 Pct Recovery = 94% Analysis Date = 10/29/17 Pct Recovery = 94% Analysis Date = 10/29/17 Pct Recovery = 94% Analysis Date = 10/20/17 Pct Recovery = 93% Analysis Date = 10/20/17 Pct Recovery = 93% Analysis Date = 10/10/17 Pct Recovery = 93% Analysis Date = 10/10/17 Pct Recovery = 93% Analysis Date = 10/01/17 Pct Recovery = 93% Analysis Date = 10/01/17 Pct Recovery = 93% Analysis Date = 09/22/17 Pct Recovery = 93% Analysis Date = 09/22/17 Pct Recovery = 93% Analysis Date = 09/13/17 Pct Recovery = 93% Analysis Date = 09/13/17 Pct Recovery = 93% Analysis Date = 09/03/17 Pct Recovery = 93% Analysis Date = 09/03/17 Pct Recovery = 93% Analysis Date = 08/25/17 Pct Recovery = 93% Analysis Date = 08/25/17 Pct Recovery = 93% Analysis Date = 08/16/17 Pct Recovery = 92% Analysis Date = 08/16/17 Pct Recovery = 92% Analysis Date = 08/07/17 Pct Recovery = 92% Analysis Date = 08/07/17 Pct Recovery = 92% Analysis Date = 07/28/17 Pct Recovery = 92% Analysis Date = 07/28/17 Pct Recovery = 92% Analysis Date = 07/19/17 Pct Recovery = 92% Analysis Date = 07/19/17 Pct Recovery = 92% Analysis Date = 07/10/17 Pct Recovery = 92% Analysis Date = 07/10/17 Pct Recovery = 92% Analysis Date = 07/01/17 Pct Recovery = 92% Analysis Date = 07/01/17 Pct Recovery = 92% Analysis Date = 06/22/17 Pct Recovery = 92% Analysis Date = 06/22/17 Pct Recovery = 92% Analysis Date = 06/12/17 Pct Recovery = 91% Analysis Date = 06/12/17 Pct Recovery = 91% Analysis Date = 06/03/17 Pct Recovery = 91% Analysis Date = 06/03/17 Pct Recovery = 91% Analysis Date = 05/25/17 Pct Recovery = 91% Analysis Date = 05/25/17 Pct Recovery = 91% Analysis Date = 05/16/17 Pct Recovery = 91% Analysis Date = 05/16/17 Pct Recovery = 91% Analysis Date = 05/06/17 Pct Recovery = 91% Analysis Date = 05/06/17 Pct Recovery = 91% Analysis Date = 04/27/17 Pct Recovery = 91% Analysis Date = 04/27/17 Pct Recovery = 91% Analysis Date = 04/18/17 Pct Recovery = 90% Analysis Date = 04/18/17 Pct Recovery = 90% Analysis Date = 04/09/17 Pct Recovery = 90% Analysis Date = 04/09/17 Pct Recovery = 90% Analysis Date = 03/30/17 Pct Recovery = 90% Analysis Date = 03/30/17 Pct Recovery = 90% Analysis Date = 03/21/17 Pct Recovery = 90% Analysis Date = 03/21/17 Pct Recovery = 90% Analysis Date = 03/12/17 Pct Recovery = 90% Analysis Date = 03/12/17 Pct Recovery = 90% Analysis Date = 03/03/17 Pct Recovery = 90% Analysis Date = 03/03/17 Pct Recovery = 90% Analysis Date = 02/21/17 Pct Recovery = 90% Analysis Date = 02/21/17 Pct Recovery = 90% Analysis Date = 02/12/17 Pct Recovery = 89% Analysis Date = 02/12/17 Pct Recovery = 89% Analysis Date = 02/03/17 Pct Recovery = 89% Analysis Date = 02/03/17 Pct Recovery = 89% Analysis Date = 01/25/17 Pct Recovery = 89% Analysis Date = 01/25/17 Pct Recovery = 89% Analysis Date = 01/15/17 Pct Recovery = 89% Analysis Date = 01/15/17 Pct Recovery = 89% Analysis Date = 01/06/17 Pct Recovery = 89% Analysis Date = 01/06/17 Pct Recovery = 89% Analysis Date = 12/28/16 Pct Recovery = 89% Analysis Date = 12/28/16 Pct Recovery = 89% Analysis Date = 12/19/16 Pct Recovery = 88% Analysis Date = 12/19/16 Pct Recovery = 88% Analysis Date = 12/09/16 Pct Recovery = 88% Analysis Date = 12/09/16 Pct Recovery = 88% Analysis Date = 11/30/16 Pct Recovery = 88% Analysis Date = 11/30/16 Pct Recovery = 88% Analysis Date = 11/21/16 Pct Recovery = 88% Analysis Date = 11/21/16 Pct Recovery = 88% Analysis Date = 11/12/16 Pct Recovery = 88% Analysis Date = 11/12/16 Pct Recovery = 88% Analysis Date = 11/03/16 Pct Recovery = 88% Analysis Date = 11/03/16 Pct Recovery = 88% Analysis Date = 10/24/16 Pct Recovery = 87% Analysis Date = 10/24/16 Pct Recovery = 87% Analysis Date = 10/15/16 Pct Recovery = 87% Analysis Date = 10/15/16 Pct Recovery = 87% Analysis Date = 10/06/16 Pct Recovery = 87% Analysis Date = 10/06/16 Pct Recovery = 87% Analysis Date = 09/27/16 Pct Recovery = 87% Analysis Date = 09/27/16 Pct Recovery = 87% Analysis Date = 09/17/16 Pct Recovery = 87% Analysis Date = 09/17/16 Pct Recovery = 87% Analysis Date = 09/08/16 Pct Recovery = 87% Analysis Date = 09/08/16 Pct Recovery = 87% Analysis Date = 08/30/16 Pct Recovery = 86% Analysis Date = 08/30/16 Pct Recovery = 86% Analysis Date = 08/21/16 Pct Recovery = 86% Analysis Date = 08/21/16 Pct Recovery = 86% Analysis Date = 08/11/16 Pct Recovery = 86% Analysis Date = 08/11/16 Pct Recovery = 86% Analysis Date = 08/02/16 Pct Recovery = 86% Analysis Date = 08/02/16 Pct Recovery = 86% Analysis Date = 07/24/16 Pct Recovery = 86% Analysis Date = 07/24/16 Pct Recovery = 86% Analysis Date = 07/15/16 Pct Recovery = 86% Analysis Date = 07/15/16 Pct Recovery = 86% Analysis Date = 07/05/16 Pct Recovery = 85% Analysis Date = 07/05/16 Pct Recovery = 85% Analysis Date = 06/26/16 Pct Recovery = 85% Analysis Date = 06/26/16 Pct Recovery = 85% Analysis Date = 06/17/16 Pct Recovery = 85% Analysis Date = 06/17/16 Pct Recovery = 85% Analysis Date = 06/08/16 Pct Recovery = 85% Analysis Date = 06/08/16 Pct Recovery = 85% Analysis Date = 05/29/16 Pct Recovery = 85% Analysis Date = 05/29/16 Pct Recovery = 85% Analysis Date = 05/20/16 Pct Recovery = 85% Analysis Date = 05/20/16 Pct Recovery = 85% Analysis Date = 05/11/16 Pct Recovery = 84% Analysis Date = 05/11/16 Pct Recovery = 84% Analysis Date = 05/02/16 Pct Recovery = 84% Analysis Date = 05/02/16 Pct Recovery = 84% Analysis Date = 04/22/16 Pct Recovery = 84% Analysis Date = 04/22/16 Pct Recovery = 84% Analysis Date = 04/13/16 Pct Recovery = 84% Analysis Date = 04/13/16 Pct Recovery = 84% Analysis Date = 04/04/16 Pct Recovery = 84% Analysis Date = 04/04/16 Pct Recovery = 84% Analysis Date = 03/26/16 Pct Recovery = 84% Analysis Date = 03/26/16 Pct Recovery = 84% Analysis Date = 03/17/16 Pct Recovery = 83% Analysis Date = 03/17/16 Pct Recovery = 83% Analysis Date = 03/07/16 Pct Recovery = 83% Analysis Date = 03/07/16 Pct Recovery = 83% Analysis Date = 02/27/16 Pct Recovery = 83% Analysis Date = 02/27/16 Pct Recovery = 83% Analysis Date = 02/18/16 Pct Recovery = 83% Analysis Date = 02/18/16 Pct Recovery = 83% Analysis Date = 02/09/16 Pct Recovery = 83% Analysis Date = 02/09/16 Pct Recovery = 83% Analysis Date = 01/30/16 Pct Recovery = 83% Analysis Date = 01/30/16 Pct Recovery = 83% Analysis Date = 01/21/16 Pct Recovery = 82% Analysis Date = 01/21/16 Pct Recovery = 82% Analysis Date = 01/12/16 Pct Recovery = 82% Analysis Date = 01/12/16 Pct Recovery = 82% Analysis Date = 01/03/16 Pct Recovery = 82% Analysis Date = 01/03/16 Pct Recovery = 82% Analysis Date = 12/24/15 Pct Recovery = 82% Analysis Date = 12/24/15 Pct Recovery = 82% Analysis Date = 12/15/15 Pct Recovery = 82% Analysis Date = 12/15/15 Pct Recovery = 82% Analysis Date = 12/06/15 Pct Recovery = 82% Analysis Date = 12/06/15 Pct Recovery = 82% Analysis Date = 11/27/15 Pct Recovery = 82% Analysis Date = 11/27/15 Pct Recovery = 82% Analysis Date = 11/17/15 Pct Recovery = 81% Analysis Date = 11/17/15 Pct Recovery = 81% Analysis Date = 11/08/15 Pct Recovery = 81% Analysis Date = 11/08/15 Pct Recovery = 81% Analysis Date = 10/30/15 Pct Recovery = 81% Analysis Date = 10/30/15 Pct Recovery = 81% Analysis Date = 10/21/15 Pct Recovery = 81% Analysis Date = 10/21/15 Pct Recovery = 81% Analysis Date = 10/11/15 Pct Recovery = 81% Analysis Date = 10/11/15 Pct Recovery = 81% Analysis Date = 10/02/15 Pct Recovery = 81% Analysis Date = 10/02/15 Pct Recovery = 81% Analysis Date = 09/23/15 Pct Recovery = 81% Analysis Date = 09/23/15 Pct Recovery = 81% Analysis Date = 09/14/15 Pct Recovery = 81% Analysis Date = 09/14/15 Pct Recovery = 81% Analysis Date = 09/04/15 Pct Recovery = 80% Analysis Date = 09/04/15 Pct Recovery = 80% Analysis Date = 08/26/15 Pct Recovery = 80% Analysis Date = 08/26/15 Pct Recovery = 80% Analysis Date = 08/17/15 Pct Recovery = 80% Analysis Date = 08/17/15 Pct Recovery = 80% Analysis Date = 08/08/15 Pct Recovery = 80% Analysis Date = 08/08/15 Pct Recovery = 80% Analysis Date = 07/30/15 Pct Recovery = 80% Analysis Date = 07/30/15 Pct Recovery = 80% Analysis Date = 07/20/15 Pct Recovery = 80% Analysis Date = 07/20/15 Pct Recovery = 80% Analysis Date = 07/11/15 Pct Recovery = 80% Analysis Date = 07/11/15 Pct Recovery = 80% Analysis Date = 07/02/15 Pct Recovery = 80% Analysis Date = 07/02/15 Pct Recovery = 80% Analysis Date = 06/23/15 Pct Recovery = 80% Analysis Date = 06/23/15 Pct Recovery = 80% Analysis Date = 06/13/15 Pct Recovery = 80% Analysis Date = 06/13/15 Pct Recovery = 80% Analysis Date = 06/04/15 Pct Recovery = 80% Analysis Date = 06/04/15 Pct Recovery = 80% Analysis Date = 05/26/15 Pct Recovery = 80% Analysis Date = 05/26/15 Pct Recovery = 80% Analysis Date = 05/17/15 Pct Recovery = 79% Analysis Date = 05/17/15 Pct Recovery = 79% Analysis Date = 05/07/15 Pct Recovery = 79% Analysis Date = 05/07/15 Pct Recovery = 79% Analysis Date = 04/28/15 Pct Recovery = 79% Analysis Date = 04/28/15 Pct Recovery = 79% Analysis Date = 04/19/15 Pct Recovery = 79% Analysis Date = 04/19/15 Pct Recovery = 79% Analysis Date = 04/10/15 Pct Recovery = 79% Analysis Date = 04/10/15 Pct Recovery = 79% Analysis Date = 03/31/15 Pct Recovery = 79% Analysis Date = 03/31/15 Pct Recovery = 79% Analysis Date = 03/22/15 Pct Recovery = 79% Analysis Date = 03/22/15 Pct Recovery = 79% Analysis Date = 03/13/15 Pct Recovery = 79% Analysis Date = 03/13/15 Pct Recovery = 79% Analysis Date = 03/04/15 Pct Recovery = 79% Analysis Date = 03/04/15 Pct Recovery = 79% Analysis Date = 02/22/15 Pct Recovery = 79% Analysis Date = 02/22/15 Pct Recovery = 79% Analysis Date = 02/13/15 Pct Recovery = 79% Analysis Date = 02/13/15 Pct Recovery = 79% Analysis Date = 02/04/15 Pct Recovery = 79% Analysis Date = 02/04/15 Pct Recovery = 79% Analysis Date = 01/26/15 Pct Recovery = 79% Analysis Date = 01/26/15 Pct Recovery = 79% Analysis Date = 01/16/15 Pct Recovery = 79% Analysis Date = 01/16/15 Pct Recovery = 79% Analysis Date = 01/07/15 Pct Recovery = 79% Analysis Date = 01/07/15 Pct Recovery = 79% Analysis Date = 12/29/14 Pct Recovery = 79% Analysis Date = 12/29/14 Pct Recovery = 79% Analysis Date = 12/20/14 Pct Recovery = 80% Analysis Date = 12/20/14 Pct Recovery = 80% Analysis Date = 12/11/14 Pct Recovery = 80% Analysis Date = 12/11/14 Pct Recovery = 80% Analysis Date = 12/01/14 Pct Recovery = 80% Analysis Date = 12/01/14 Pct Recovery = 80% Analysis Date = 11/22/14 Pct Recovery = 80% Analysis Date = 11/22/14 Pct Recovery = 80% Analysis Date = 11/13/14 Pct Recovery = 80% Analysis Date = 11/13/14 Pct Recovery = 80% Analysis Date = 11/04/14 Pct Recovery = 80% Analysis Date = 11/04/14 Pct Recovery = 80% Analysis Date = 10/25/14 Pct Recovery = 80% Analysis Date = 10/25/14 Pct Recovery = 80% Analysis Date = 10/16/14 Pct Recovery = 80% Analysis Date = 10/16/14 Pct Recovery = 80% Analysis Date = 10/07/14 Pct Recovery = 80% Analysis Date = 10/07/14 Pct Recovery = 80% Analysis Date = 09/28/14 Pct Recovery = 80% Analysis Date = 09/28/14 Pct Recovery = 80% Analysis Date = 09/18/14 Pct Recovery = 80% Analysis Date = 09/18/14 Pct Recovery = 80% Analysis Date = 09/09/14 Pct Recovery = 80% Analysis Date = 09/09/14 Pct Recovery = 80% Analysis Date = 08/31/14 Pct Recovery = 80% Analysis Date = 08/31/14 Pct Recovery = 80% Analysis Date = 08/22/14 Pct Recovery = 80% Analysis Date = 08/22/14 Pct Recovery = 80% Analysis Date = 08/12/14 Pct Recovery = 81% Analysis Date = 08/12/14 Pct Recovery = 81% Analysis Date = 08/03/14 Pct Recovery = 81% Analysis Date = 08/03/14 Pct Recovery = 81% Analysis Date = 07/25/14 Pct Recovery = 81% Analysis Date = 07/25/14 Pct Recovery = 81% Analysis Date = 07/16/14 Pct Recovery = 81% Analysis Date = 07/16/14 Pct Recovery = 81% Analysis Date = 07/06/14 Pct Recovery = 81% Analysis Date = 07/06/14 Pct Recovery = 81% Analysis Date = 06/27/14 Pct Recovery = 81% Analysis Date = 06/27/14 Pct Recovery = 81% Analysis Date = 06/18/14 Pct Recovery = 81% Analysis Date = 06/18/14 Pct Recovery = 81% Analysis Date = 06/09/14 Pct Recovery = 81% Analysis Date = 06/09/14 Pct Recovery = 81% Analysis Date = 05/30/14 Pct Recovery = 81% Analysis Date = 05/30/14 Pct Recovery = 81% Analysis Date = 05/21/14 Pct Recovery = 81% Analysis Date = 05/21/14 Pct Recovery = 81% Analysis Date = 05/12/14 Pct Recovery = 81% Analysis Date = 05/12/14 Pct Recovery = 81% Analysis Date = 05/03/14 Pct Recovery = 82% Analysis Date = 05/03/14 Pct Recovery = 82% Analysis Date = 04/24/14 Pct Recovery = 82% Analysis Date = 04/24/14 Pct Recovery = 82% Analysis Date = 04/14/14 Pct Recovery = 82% Analysis Date = 04/14/14 Pct Recovery = 82% Analysis Date = 04/05/14 Pct Recovery = 82% Analysis Date = 04/05/14 Pct Recovery = 82% Analysis Date = 03/27/14 Pct Recovery = 82% Analysis Date = 03/27/14 Pct Recovery = 82% Analysis Date = 03/18/14 Pct Recovery = 82% Analysis Date = 03/18/14 Pct Recovery = 82% Analysis Date = 03/08/14 Pct Recovery = 82% Analysis Date = 03/08/14 Pct Recovery = 82% Analysis Date = 02/27/14 Pct Recovery = 82% Analysis Date = 02/27/14 Pct Recovery = 82% Analysis Date = 02/18/14 Pct Recovery = 82% Analysis Date = 02/18/14 Pct Recovery = 82% Analysis Date = 02/09/14 Pct Recovery = 83% Analysis Date = 02/09/14 Pct Recovery = 83% Analysis Date = 01/30/14 Pct Recovery = 83% Analysis Date = 01/30/14 Pct Recovery = 83% Analysis Date = 01/21/14 Pct Recovery = 83% Analysis Date = 01/21/14 Pct Recovery = 83% Analysis Date = 01/12/14 Pct Recovery = 83% Analysis Date = 01/12/14 Pct Recovery = 83% Analysis Date = 01/03/14 Pct Recovery = 83% Analysis Date = 01/03/14 Pct Recovery = 83% Analysis Date = 12/24/13 Pct Recovery = 83% Analysis Date = 12/24/13 Pct Recovery = 83% Analysis Date = 12/15/13 Pct Recovery = 83% Analysis Date = 12/15/13 Pct Recovery = 83% Analysis Date = 12/06/13 Pct Recovery = 83% Analysis Date = 12/06/13 Pct Recovery = 83% Analysis Date = 11/27/13 Pct Recovery = 83% Analysis Date = 11/27/13 Pct Recovery = 83% Analysis Date = 11/17/13 Pct Recovery = 83% Analysis Date = 11/17/13 Pct Recovery = 83% Analysis Date = 11/08/13 Pct Recovery = 84% Analysis Date = 11/08/13 Pct Recovery = 84% Analysis Date = 10/30/13 Pct Recovery = 84% Analysis Date = 10/30/13 Pct Recovery = 84% Analysis Date = 10/21/13 Pct Recovery = 84% Analysis Date = 10/21/13 Pct Recovery = 84% Analysis Date = 10/11/13 Pct Recovery = 84% Analysis Date = 10/11/13 Pct Recovery = 84% Analysis Date = 10/02/13 Pct Recovery = 84% Analysis Date = 10/02/13 Pct Recovery = 84% Analysis Date = 09/23/13 Pct Recovery = 84% Analysis Date = 09/23/13 Pct Recovery = 84% Analysis Date = 09/14/13 Pct Recovery = 84% Analysis Date = 09/14/13 Pct Recovery = 84% Analysis Date = 09/05/13 Pct Recovery = 84% Analysis Date = 09/05/13 Pct Recovery = 84% Analysis Date = 08/26/13 Pct Recovery = 84% Analysis Date = 08/26/13 Pct Recovery = 84% Analysis Date = 08/17/13 Pct Recovery = 84% Analysis Date = 08/17/13 Pct Recovery = 84% Analysis Date = 08/08/13 Pct Recovery = 84% Analysis Date = 08/08/13 Pct Recovery = 84% Analysis Date = 07/30/13 Pct Recovery = 84% Analysis Date = 07/30/13 Pct Recovery = 84% Analysis Date = 07/20/13 Pct Recovery = 85% Analysis Date = 07/20/13 Pct Recovery = 85% Analysis Date = 07/11/13 Pct Recovery = 85% Analysis Date = 07/11/13 Pct Recovery = 85% Analysis Date = 07/02/13 Pct Recovery = 85% Analysis Date = 07/02/13 Pct Recovery = 85% Analysis Date = 06/23/13 Pct Recovery = 85% Analysis Date = 06/23/13 Pct Recovery = 85% Analysis Date = 06/13/13 Pct Recovery = 85% Analysis Date = 06/13/13 Pct Recovery = 85% Analysis Date = 06/04/13 Pct Recovery = 85% Analysis Date = 06/04/13 Pct Recovery = 85% Analysis Date = 05/26/13 Pct Recovery = 85% Analysis Date = 05/26/13 Pct Recovery = 85% Analysis Date = 05/17/13 Pct Recovery = 85% Analysis Date = 05/17/13 Pct Recovery = 85% Analysis Date = 05/07/13 Pct Recovery = 85% Analysis Date = 05/07/13 Pct Recovery = 85% Analysis Date = 04/28/13 Pct Recovery = 85% Analysis Date = 04/28/13 Pct Recovery = 85% Analysis Date = 04/19/13 Pct Recovery = 85% Analysis Date = 04/19/13 Pct Recovery = 85% Analysis Date = 04/10/13 Pct Recovery = 85% Analysis Date = 04/10/13 Pct Recovery = 85% Analysis Date = 03/31/13 Pct Recovery = 85% Analysis Date = 03/31/13 Pct Recovery = 85% Analysis Date = 03/22/13 Pct Recovery = 86% Analysis Date = 03/22/13 Pct Recovery = 86% Analysis Date = 03/13/13 Pct Recovery = 86% Analysis Date = 03/13/13 Pct Recovery = 86% Analysis Date = 03/04/13 Pct Recovery = 86% Analysis Date = 03/04/13 Pct Recovery = 86% Analysis Date = 02/22/13 Pct Recovery = 86% Analysis Date = 02/22/13 Pct Recovery = 86% Analysis Date = 02/13/13 Pct Recovery = 86% Analysis Date = 02/13/13 Pct Recovery = 86% Analysis Date = 02/04/13 Pct Recovery = 86% Analysis Date = 02/04/13 Pct Recovery = 86% Analysis Date = 01/26/13 Pct Recovery = 86% Analysis Date = 01/26/13 Pct Recovery = 86% Analysis Date = 01/17/13 Pct Recovery = 86% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
METOLACHLOR

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 78 84% 13% 84% 13%
Total 78 84% 13% 84% 13%

Sample Statistics
METOLACHLOR

Characteristic N % % Basis
Plotted 78 100% Spiked
Estimated Values 4 5% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 78 .  
False Negatives 0 0% 0 out of 78
Not Spiked 40 .  
False Positives 0 0% 0 out of 40

OBSP Determination:
METRIBUZIN
METHOD: 2033 , TESTIDCODE: 82630GCM35

Laboratory ID = 20132490342 Lab Value = 0.124 Expected Conc. = 0.2 Report level label = 0.012 Pct Recovery = 62% Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20140370077 Lab Value = 0.058 Expected Conc. = 0.1 Report level label = 0.012 Pct Recovery = 58% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20132560001 Lab Value = 0.065 Expected Conc. = 0.1 Report level label = 0.012 Pct Recovery = 65% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20132140002 Lab Value = 0.075 Expected Conc. = 0.1 Report level label = 0.012 Pct Recovery = 75% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl SpecificMix = LB99392 Laboratory ID = 20131370001 Lab Value = 0.096 Expected Conc. = 0.1 Report level label = 0.012 Pct Recovery = 96% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl SpecificMix = LB99392 Laboratory ID = 20172510330 Lab Value = 0.055 Expected Conc. = 0.08 Report level label = 0.012 Pct Recovery = 69% Analysis Date = 12/29/17 SpikeMix = ChemService 6537100: 100 µl & Abs 071817Pest: 100 µl SpecificMix = 071817Pest Laboratory ID = 20130940097 Lab Value = 0.049 Expected Conc. = 0.076 Report level label = 0.012 Pct Recovery = 64% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = 0507-12-04.2 Laboratory ID = 20123560092 Lab Value = 0.060 Expected Conc. = 0.076 Report level label = 0.012 Pct Recovery = 79% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = 0507-12-04.2 Laboratory ID = 20163370001 Lab Value = 0.057 Expected Conc. = 0.075 Report level label = 0.012 Pct Recovery = 75% Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl SpecificMix = B20160331 Laboratory ID = 20163150006 Lab Value = 0.049 Expected Conc. = 0.075 Report level label = 0.012 Pct Recovery = 65% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl SpecificMix = B20160331 Laboratory ID = 20161880109 Lab Value = 0.057 Expected Conc. = 0.075 Report level label = 0.012 Pct Recovery = 76% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl SpecificMix = 03FF076 Laboratory ID = 20130810108 Lab Value = 0.066 Expected Conc. = 0.075 Report level label = 0.012 Pct Recovery = 88% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl SpecificMix = LB92783 Laboratory ID = 20130100066 Lab Value = 0.061 Expected Conc. = 0.075 Report level label = 0.012 Pct Recovery = 81% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl SpecificMix = LB92783 Laboratory ID = 20152610011 Lab Value = 0.020 Expected Conc. = 0.0723 Report level label = 0.012 Pct Recovery = 28% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl SpecificMix = 0406-15-01 Laboratory ID = 20152460215 Lab Value = 0.045 Expected Conc. = 0.0723 Report level label = 0.012 Pct Recovery = 63% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl SpecificMix = 0406-15-01 Laboratory ID = 20171720140 Lab Value = 0.050 Expected Conc. = 0.06 Report level label = 0.012 Pct Recovery = 84% Analysis Date = 08/31/17 SpikeMix = Supelco LC20138V: 80 µl & Phenova B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20171660002 Lab Value = 0.049 Expected Conc. = 0.06 Report level label = 0.012 Pct Recovery = 81% Analysis Date = 08/23/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20170960001 Lab Value = 0.044 Expected Conc. = 0.06 Report level label = 0.012 Pct Recovery = 73% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl SpecificMix = 03FF076 Laboratory ID = 20170190026 Lab Value = 0.041 Expected Conc. = 0.06 Report level label = 0.012 Pct Recovery = 68% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20161470001 Lab Value = 0.046 Expected Conc. = 0.06 Report level label = 0.012 Pct Recovery = 77% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20150430092 Lab Value = 0.013 Expected Conc. = 0.048 Report level label = 0.012 Pct Recovery = 27% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl SpecificMix = E1140407002 Laboratory ID = 20143240095 Lab Value = 0.042 Expected Conc. = 0.048 Report level label = 0.012 Pct Recovery = 86% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl SpecificMix = 032714 Laboratory ID = 20143110108 Lab Value = 0.036 Expected Conc. = 0.048 Report level label = 0.012 Pct Recovery = 76% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl SpecificMix = E1140407002 Laboratory ID = 20142720002 Lab Value = 0.034 Expected Conc. = 0.048 Report level label = 0.012 Pct Recovery = 70% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl SpecificMix = E1140407002 Laboratory ID = 20142270001 Lab Value = 0.031 Expected Conc. = 0.048 Report level label = 0.012 Pct Recovery = 64% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl SpecificMix = 032714 Laboratory ID = 20141770149 Lab Value = 0.032 Expected Conc. = 0.048 Report level label = 0.012 Pct Recovery = 66% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl SpecificMix = E1140407002 Laboratory ID = 20141220025 Lab Value = 0.048 Expected Conc. = 0.048 Report level label = 0.012 Pct Recovery = 101% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl SpecificMix = 032714 Laboratory ID = 20181430122 Lab Value = 0.036 Expected Conc. = 0.04 Report level label = 0.012 Pct Recovery = 90% Analysis Date = 06/20/18 SpikeMix = Abs 071817Pest: 50 µl & Spex Organics EN170808006: 50 µl SpecificMix = 071817Pest Laboratory ID = 20173480003 Lab Value = 0.031 Expected Conc. = 0.04 Report level label = 0.012 Pct Recovery = 76% Analysis Date = 04/05/18 SpikeMix = Abs 071717Pest: 50 µl & ChemService 6567600: 50 µl SpecificMix = 6567600 Laboratory ID = 20172560101 Lab Value = 0.027 Expected Conc. = 0.04 Report level label = 0.012 Pct Recovery = 69% Analysis Date = 12/22/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6567600: 50 µl SpecificMix = 6567600 Laboratory ID = 20140510043 Lab Value = 0.023 Expected Conc. = 0.04 Report level label = 0.012 Pct Recovery = 59% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl SpecificMix = LB99392 Laboratory ID = 20133580036 Lab Value = 0.021 Expected Conc. = 0.04 Report level label = 0.012 Pct Recovery = 53% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20133470008 Lab Value = 0.038 Expected Conc. = 0.04 Report level label = 0.012 Pct Recovery = 94% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl SpecificMix = LB99392 Laboratory ID = 20133190012 Lab Value = 0.046 Expected Conc. = 0.04 Report level label = 0.012 Pct Recovery = 116% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = LB99392 Laboratory ID = 20133050050 Lab Value = 0.040 Expected Conc. = 0.04 Report level label = 0.012 Pct Recovery = 100% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl SpecificMix = LB99392 Laboratory ID = 20131790009 Lab Value = 0.024 Expected Conc. = 0.04 Report level label = 0.012 Pct Recovery = 59% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20131510026 Lab Value = 0.027 Expected Conc. = 0.04 Report level label = 0.012 Pct Recovery = 68% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20160770090 Lab Value = 0.029 Expected Conc. = 0.0362 Report level label = 0.012 Pct Recovery = 80% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20160630046 Lab Value = 0.025 Expected Conc. = 0.0362 Report level label = 0.012 Pct Recovery = 69% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20153510109 Lab Value = 0.028 Expected Conc. = 0.0362 Report level label = 0.012 Pct Recovery = 77% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20153440001 Lab Value = 0.032 Expected Conc. = 0.0362 Report level label = 0.012 Pct Recovery = 87% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20161260151 Lab Value = 0.026 Expected Conc. = 0.036 Report level label = 0.012 Pct Recovery = 71% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = 3851600 Laboratory ID = 20151550293 Lab Value = 0.034 Expected Conc. = 0.036 Report level label = 0.012 Pct Recovery = 93% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl SpecificMix = 3851600 Laboratory ID = 20151270112 Lab Value = 0.030 Expected Conc. = 0.036 Report level label = 0.012 Pct Recovery = 83% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl SpecificMix = 3851600 Laboratory ID = 20130510051 Lab Value = 0.022 Expected Conc. = 0.0304 Report level label = 0.012 Pct Recovery = 73% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl SpecificMix = 0507-12-04.2 Laboratory ID = 20172020035 Lab Value = 0.030 Expected Conc. = 0.03 Report level label = 0.012 Pct Recovery = 101% Analysis Date = 11/07/17 SpikeMix = Abs 071717Pest: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20171510080 Lab Value = 0.026 Expected Conc. = 0.03 Report level label = 0.012 Pct Recovery = 88% Analysis Date = 06/09/17 SpikeMix = Supelco LC20138V: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20171160110 Lab Value = 0.024 Expected Conc. = 0.03 Report level label = 0.012 Pct Recovery = 81% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = B20160331 Laboratory ID = 20170460061 Lab Value = 0.023 Expected Conc. = 0.03 Report level label = 0.012 Pct Recovery = 76% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl SpecificMix = 03FF076 Laboratory ID = 20162660005 Lab Value = 0.019 Expected Conc. = 0.03 Report level label = 0.012 Pct Recovery = 64% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl SpecificMix = 03FF076 Laboratory ID = 20162380004 Lab Value = 0.023 Expected Conc. = 0.03 Report level label = 0.012 Pct Recovery = 77% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = B20160331 Laboratory ID = 20162150213 Lab Value = 0.026 Expected Conc. = 0.03 Report level label = 0.012 Pct Recovery = 85% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl SpecificMix = B20160331 Laboratory ID = 20161600087 Lab Value = 0.025 Expected Conc. = 0.03 Report level label = 0.012 Pct Recovery = 84% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20161340228 Lab Value = 0.022 Expected Conc. = 0.03 Report level label = 0.012 Pct Recovery = 73% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl SpecificMix = 03FF076 Laboratory ID = 20161190075 Lab Value = 0.021 Expected Conc. = 0.03 Report level label = 0.012 Pct Recovery = 69% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20130390105 Lab Value = 0.021 Expected Conc. = 0.03 Report level label = 0.012 Pct Recovery = 70% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl SpecificMix = LB92783 Laboratory ID = 20180730064 Lab Value = 0.022 Expected Conc. = 0.024 Report level label = 0.012 Pct Recovery = 91% Analysis Date = 05/16/18 SpikeMix = Abs 071717Pest: 30 µl & Abs 071817Pest: 30 µl SpecificMix = 071817Pest Laboratory ID = 20180050004 Lab Value = 0.022 Expected Conc. = 0.024 Report level label = 0.012 Pct Recovery = 93% Analysis Date = 04/05/18 SpikeMix = Abs 071817Pest: 30 µl & ChemService 6472100: 30 µl SpecificMix = 071817Pest Laboratory ID = 20172780018 Lab Value = 0.019 Expected Conc. = 0.024 Report level label = 0.012 Pct Recovery = 77% Analysis Date = 02/08/18 SpikeMix = ChemService 6537100: 30 µl & Abs 071817Pest: 30 µl SpecificMix = 071817Pest Laboratory ID = 20150150115 Lab Value = 0.025 Expected Conc. = 0.024 Report level label = 0.012 Pct Recovery = 104% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl SpecificMix = 032714 Laboratory ID = 20142820151 Lab Value = 0.019 Expected Conc. = 0.024 Report level label = 0.012 Pct Recovery = 78% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl SpecificMix = 032714 Laboratory ID = 20142470041 Lab Value = 0.022 Expected Conc. = 0.024 Report level label = 0.012 Pct Recovery = 92% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141910243 Lab Value = 0.017 Expected Conc. = 0.024 Report level label = 0.012 Pct Recovery = 71% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141640076 Lab Value = 0.019 Expected Conc. = 0.024 Report level label = 0.012 Pct Recovery = 81% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141490205 Lab Value = 0.022 Expected Conc. = 0.024 Report level label = 0.012 Pct Recovery = 93% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = 032714 Laboratory ID = 20141360094 Lab Value = 0.019 Expected Conc. = 0.024 Report level label = 0.012 Pct Recovery = 79% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141080004 Lab Value = 0.022 Expected Conc. = 0.024 Report level label = 0.012 Pct Recovery = 93% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl SpecificMix = 032714 Laboratory ID = 20152190003 Lab Value = 0.013 Expected Conc. = 0.0181 Report level label = 0.012 Pct Recovery = 73% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = 0406-15-01 Laboratory ID = 20152040177 Lab Value = 0.021 Expected Conc. = 0.0181 Report level label = 0.012 Pct Recovery = 116% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl SpecificMix = 0406-15-01 Laboratory ID = 20160430111 Lab Value = 0.016 Expected Conc. = 0.018 Report level label = 0.012 Pct Recovery = 91% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 3851600 Laboratory ID = 20160210080 Lab Value = 0.012 Expected Conc. = 0.018 Report level label = 0.012 Pct Recovery = 67% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 3851600 Laboratory ID = 20152950078 Lab Value = 0.011 Expected Conc. = 0.018 Report level label = 0.012 Pct Recovery = 62% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 3851600 Laboratory ID = 20153030068 Lab Value = 0.015 Expected Conc. = 0.018 Report level label = 0.012 Pct Recovery = 83% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = 3851600 Laboratory ID = 20151760208 Lab Value = 0.021 Expected Conc. = 0.018 Report level label = 0.012 Pct Recovery = 119% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl SpecificMix = 3851600 Laboratory ID = 20151380009 Lab Value = 0.015 Expected Conc. = 0.018 Report level label = 0.012 Pct Recovery = 86% Analysis Date = 05/30/15 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 3851600 Analysis Date = 06/19/18 Pct Recovery = 83% Analysis Date = 06/10/18 Pct Recovery = 83% Analysis Date = 06/10/18 Pct Recovery = 83% Analysis Date = 05/31/18 Pct Recovery = 83% Analysis Date = 05/31/18 Pct Recovery = 83% Analysis Date = 05/21/18 Pct Recovery = 83% Analysis Date = 05/21/18 Pct Recovery = 83% Analysis Date = 05/11/18 Pct Recovery = 83% Analysis Date = 05/11/18 Pct Recovery = 83% Analysis Date = 05/01/18 Pct Recovery = 83% Analysis Date = 05/01/18 Pct Recovery = 83% Analysis Date = 04/21/18 Pct Recovery = 83% Analysis Date = 04/21/18 Pct Recovery = 83% Analysis Date = 04/11/18 Pct Recovery = 83% Analysis Date = 04/11/18 Pct Recovery = 83% Analysis Date = 04/01/18 Pct Recovery = 82% Analysis Date = 04/01/18 Pct Recovery = 82% Analysis Date = 03/22/18 Pct Recovery = 82% Analysis Date = 03/22/18 Pct Recovery = 82% Analysis Date = 03/12/18 Pct Recovery = 82% Analysis Date = 03/12/18 Pct Recovery = 82% Analysis Date = 03/02/18 Pct Recovery = 82% Analysis Date = 03/02/18 Pct Recovery = 82% Analysis Date = 02/21/18 Pct Recovery = 82% Analysis Date = 02/21/18 Pct Recovery = 82% Analysis Date = 02/11/18 Pct Recovery = 82% Analysis Date = 02/11/18 Pct Recovery = 82% Analysis Date = 02/01/18 Pct Recovery = 82% Analysis Date = 02/01/18 Pct Recovery = 82% Analysis Date = 01/22/18 Pct Recovery = 82% Analysis Date = 01/22/18 Pct Recovery = 82% Analysis Date = 01/12/18 Pct Recovery = 82% Analysis Date = 01/12/18 Pct Recovery = 82% Analysis Date = 01/02/18 Pct Recovery = 81% Analysis Date = 01/02/18 Pct Recovery = 81% Analysis Date = 12/23/17 Pct Recovery = 81% Analysis Date = 12/23/17 Pct Recovery = 81% Analysis Date = 12/13/17 Pct Recovery = 81% Analysis Date = 12/13/17 Pct Recovery = 81% Analysis Date = 12/03/17 Pct Recovery = 81% Analysis Date = 12/03/17 Pct Recovery = 81% Analysis Date = 11/23/17 Pct Recovery = 81% Analysis Date = 11/23/17 Pct Recovery = 81% Analysis Date = 11/13/17 Pct Recovery = 81% Analysis Date = 11/13/17 Pct Recovery = 81% Analysis Date = 11/04/17 Pct Recovery = 81% Analysis Date = 11/04/17 Pct Recovery = 81% Analysis Date = 10/25/17 Pct Recovery = 81% Analysis Date = 10/25/17 Pct Recovery = 81% Analysis Date = 10/15/17 Pct Recovery = 80% Analysis Date = 10/15/17 Pct Recovery = 80% Analysis Date = 10/05/17 Pct Recovery = 80% Analysis Date = 10/05/17 Pct Recovery = 80% Analysis Date = 09/25/17 Pct Recovery = 80% Analysis Date = 09/25/17 Pct Recovery = 80% Analysis Date = 09/15/17 Pct Recovery = 80% Analysis Date = 09/15/17 Pct Recovery = 80% Analysis Date = 09/05/17 Pct Recovery = 80% Analysis Date = 09/05/17 Pct Recovery = 80% Analysis Date = 08/26/17 Pct Recovery = 80% Analysis Date = 08/26/17 Pct Recovery = 80% Analysis Date = 08/16/17 Pct Recovery = 80% Analysis Date = 08/16/17 Pct Recovery = 80% Analysis Date = 08/06/17 Pct Recovery = 80% Analysis Date = 08/06/17 Pct Recovery = 80% Analysis Date = 07/27/17 Pct Recovery = 80% Analysis Date = 07/27/17 Pct Recovery = 80% Analysis Date = 07/18/17 Pct Recovery = 79% Analysis Date = 07/18/17 Pct Recovery = 79% Analysis Date = 07/08/17 Pct Recovery = 79% Analysis Date = 07/08/17 Pct Recovery = 79% Analysis Date = 06/28/17 Pct Recovery = 79% Analysis Date = 06/28/17 Pct Recovery = 79% Analysis Date = 06/18/17 Pct Recovery = 79% Analysis Date = 06/18/17 Pct Recovery = 79% Analysis Date = 06/08/17 Pct Recovery = 79% Analysis Date = 06/08/17 Pct Recovery = 79% Analysis Date = 05/29/17 Pct Recovery = 79% Analysis Date = 05/29/17 Pct Recovery = 79% Analysis Date = 05/19/17 Pct Recovery = 79% Analysis Date = 05/19/17 Pct Recovery = 79% Analysis Date = 05/09/17 Pct Recovery = 79% Analysis Date = 05/09/17 Pct Recovery = 79% Analysis Date = 04/29/17 Pct Recovery = 79% Analysis Date = 04/29/17 Pct Recovery = 79% Analysis Date = 04/19/17 Pct Recovery = 78% Analysis Date = 04/19/17 Pct Recovery = 78% Analysis Date = 04/09/17 Pct Recovery = 78% Analysis Date = 04/09/17 Pct Recovery = 78% Analysis Date = 03/31/17 Pct Recovery = 78% Analysis Date = 03/31/17 Pct Recovery = 78% Analysis Date = 03/21/17 Pct Recovery = 78% Analysis Date = 03/21/17 Pct Recovery = 78% Analysis Date = 03/11/17 Pct Recovery = 78% Analysis Date = 03/11/17 Pct Recovery = 78% Analysis Date = 03/01/17 Pct Recovery = 78% Analysis Date = 03/01/17 Pct Recovery = 78% Analysis Date = 02/19/17 Pct Recovery = 78% Analysis Date = 02/19/17 Pct Recovery = 78% Analysis Date = 02/09/17 Pct Recovery = 78% Analysis Date = 02/09/17 Pct Recovery = 78% Analysis Date = 01/30/17 Pct Recovery = 78% Analysis Date = 01/30/17 Pct Recovery = 78% Analysis Date = 01/20/17 Pct Recovery = 78% Analysis Date = 01/20/17 Pct Recovery = 78% Analysis Date = 01/10/17 Pct Recovery = 77% Analysis Date = 01/10/17 Pct Recovery = 77% Analysis Date = 12/31/16 Pct Recovery = 77% Analysis Date = 12/31/16 Pct Recovery = 77% Analysis Date = 12/21/16 Pct Recovery = 77% Analysis Date = 12/21/16 Pct Recovery = 77% Analysis Date = 12/12/16 Pct Recovery = 77% Analysis Date = 12/12/16 Pct Recovery = 77% Analysis Date = 12/02/16 Pct Recovery = 77% Analysis Date = 12/02/16 Pct Recovery = 77% Analysis Date = 11/22/16 Pct Recovery = 77% Analysis Date = 11/22/16 Pct Recovery = 77% Analysis Date = 11/12/16 Pct Recovery = 77% Analysis Date = 11/12/16 Pct Recovery = 77% Analysis Date = 11/02/16 Pct Recovery = 77% Analysis Date = 11/02/16 Pct Recovery = 77% Analysis Date = 10/23/16 Pct Recovery = 77% Analysis Date = 10/23/16 Pct Recovery = 77% Analysis Date = 10/13/16 Pct Recovery = 77% Analysis Date = 10/13/16 Pct Recovery = 77% Analysis Date = 10/03/16 Pct Recovery = 77% Analysis Date = 10/03/16 Pct Recovery = 77% Analysis Date = 09/23/16 Pct Recovery = 77% Analysis Date = 09/23/16 Pct Recovery = 77% Analysis Date = 09/13/16 Pct Recovery = 77% Analysis Date = 09/13/16 Pct Recovery = 77% Analysis Date = 09/03/16 Pct Recovery = 77% Analysis Date = 09/03/16 Pct Recovery = 77% Analysis Date = 08/25/16 Pct Recovery = 77% Analysis Date = 08/25/16 Pct Recovery = 77% Analysis Date = 08/15/16 Pct Recovery = 77% Analysis Date = 08/15/16 Pct Recovery = 77% Analysis Date = 08/05/16 Pct Recovery = 77% Analysis Date = 08/05/16 Pct Recovery = 77% Analysis Date = 07/26/16 Pct Recovery = 77% Analysis Date = 07/26/16 Pct Recovery = 77% Analysis Date = 07/16/16 Pct Recovery = 77% Analysis Date = 07/16/16 Pct Recovery = 77% Analysis Date = 07/06/16 Pct Recovery = 77% Analysis Date = 07/06/16 Pct Recovery = 77% Analysis Date = 06/26/16 Pct Recovery = 77% Analysis Date = 06/26/16 Pct Recovery = 77% Analysis Date = 06/16/16 Pct Recovery = 77% Analysis Date = 06/16/16 Pct Recovery = 77% Analysis Date = 06/06/16 Pct Recovery = 77% Analysis Date = 06/06/16 Pct Recovery = 77% Analysis Date = 05/27/16 Pct Recovery = 77% Analysis Date = 05/27/16 Pct Recovery = 77% Analysis Date = 05/17/16 Pct Recovery = 77% Analysis Date = 05/17/16 Pct Recovery = 77% Analysis Date = 05/08/16 Pct Recovery = 77% Analysis Date = 05/08/16 Pct Recovery = 77% Analysis Date = 04/28/16 Pct Recovery = 77% Analysis Date = 04/28/16 Pct Recovery = 77% Analysis Date = 04/18/16 Pct Recovery = 77% Analysis Date = 04/18/16 Pct Recovery = 77% Analysis Date = 04/08/16 Pct Recovery = 77% Analysis Date = 04/08/16 Pct Recovery = 77% Analysis Date = 03/29/16 Pct Recovery = 77% Analysis Date = 03/29/16 Pct Recovery = 77% Analysis Date = 03/19/16 Pct Recovery = 77% Analysis Date = 03/19/16 Pct Recovery = 77% Analysis Date = 03/09/16 Pct Recovery = 77% Analysis Date = 03/09/16 Pct Recovery = 77% Analysis Date = 02/28/16 Pct Recovery = 77% Analysis Date = 02/28/16 Pct Recovery = 77% Analysis Date = 02/18/16 Pct Recovery = 77% Analysis Date = 02/18/16 Pct Recovery = 77% Analysis Date = 02/08/16 Pct Recovery = 77% Analysis Date = 02/08/16 Pct Recovery = 77% Analysis Date = 01/29/16 Pct Recovery = 77% Analysis Date = 01/29/16 Pct Recovery = 77% Analysis Date = 01/20/16 Pct Recovery = 77% Analysis Date = 01/20/16 Pct Recovery = 77% Analysis Date = 01/10/16 Pct Recovery = 77% Analysis Date = 01/10/16 Pct Recovery = 77% Analysis Date = 12/31/15 Pct Recovery = 77% Analysis Date = 12/31/15 Pct Recovery = 77% Analysis Date = 12/21/15 Pct Recovery = 77% Analysis Date = 12/21/15 Pct Recovery = 77% Analysis Date = 12/11/15 Pct Recovery = 77% Analysis Date = 12/11/15 Pct Recovery = 77% Analysis Date = 12/01/15 Pct Recovery = 77% Analysis Date = 12/01/15 Pct Recovery = 77% Analysis Date = 11/21/15 Pct Recovery = 77% Analysis Date = 11/21/15 Pct Recovery = 77% Analysis Date = 11/11/15 Pct Recovery = 78% Analysis Date = 11/11/15 Pct Recovery = 78% Analysis Date = 11/01/15 Pct Recovery = 78% Analysis Date = 11/01/15 Pct Recovery = 78% Analysis Date = 10/22/15 Pct Recovery = 78% Analysis Date = 10/22/15 Pct Recovery = 78% Analysis Date = 10/12/15 Pct Recovery = 78% Analysis Date = 10/12/15 Pct Recovery = 78% Analysis Date = 10/02/15 Pct Recovery = 78% Analysis Date = 10/02/15 Pct Recovery = 78% Analysis Date = 09/23/15 Pct Recovery = 78% Analysis Date = 09/23/15 Pct Recovery = 78% Analysis Date = 09/13/15 Pct Recovery = 78% Analysis Date = 09/13/15 Pct Recovery = 78% Analysis Date = 09/03/15 Pct Recovery = 78% Analysis Date = 09/03/15 Pct Recovery = 78% Analysis Date = 08/24/15 Pct Recovery = 78% Analysis Date = 08/24/15 Pct Recovery = 78% Analysis Date = 08/14/15 Pct Recovery = 78% Analysis Date = 08/14/15 Pct Recovery = 78% Analysis Date = 08/04/15 Pct Recovery = 78% Analysis Date = 08/04/15 Pct Recovery = 78% Analysis Date = 07/25/15 Pct Recovery = 78% Analysis Date = 07/25/15 Pct Recovery = 78% Analysis Date = 07/15/15 Pct Recovery = 78% Analysis Date = 07/15/15 Pct Recovery = 78% Analysis Date = 07/05/15 Pct Recovery = 78% Analysis Date = 07/05/15 Pct Recovery = 78% Analysis Date = 06/25/15 Pct Recovery = 78% Analysis Date = 06/25/15 Pct Recovery = 78% Analysis Date = 06/15/15 Pct Recovery = 78% Analysis Date = 06/15/15 Pct Recovery = 78% Analysis Date = 06/06/15 Pct Recovery = 78% Analysis Date = 06/06/15 Pct Recovery = 78% Analysis Date = 05/27/15 Pct Recovery = 78% Analysis Date = 05/27/15 Pct Recovery = 78% Analysis Date = 05/17/15 Pct Recovery = 78% Analysis Date = 05/17/15 Pct Recovery = 78% Analysis Date = 05/07/15 Pct Recovery = 78% Analysis Date = 05/07/15 Pct Recovery = 78% Analysis Date = 04/27/15 Pct Recovery = 78% Analysis Date = 04/27/15 Pct Recovery = 78% Analysis Date = 04/17/15 Pct Recovery = 79% Analysis Date = 04/17/15 Pct Recovery = 79% Analysis Date = 04/07/15 Pct Recovery = 79% Analysis Date = 04/07/15 Pct Recovery = 79% Analysis Date = 03/28/15 Pct Recovery = 79% Analysis Date = 03/28/15 Pct Recovery = 79% Analysis Date = 03/18/15 Pct Recovery = 79% Analysis Date = 03/18/15 Pct Recovery = 79% Analysis Date = 03/08/15 Pct Recovery = 79% Analysis Date = 03/08/15 Pct Recovery = 79% Analysis Date = 02/26/15 Pct Recovery = 79% Analysis Date = 02/26/15 Pct Recovery = 79% Analysis Date = 02/17/15 Pct Recovery = 79% Analysis Date = 02/17/15 Pct Recovery = 79% Analysis Date = 02/07/15 Pct Recovery = 79% Analysis Date = 02/07/15 Pct Recovery = 79% Analysis Date = 01/28/15 Pct Recovery = 79% Analysis Date = 01/28/15 Pct Recovery = 79% Analysis Date = 01/18/15 Pct Recovery = 79% Analysis Date = 01/18/15 Pct Recovery = 79% Analysis Date = 01/08/15 Pct Recovery = 79% Analysis Date = 01/08/15 Pct Recovery = 79% Analysis Date = 12/29/14 Pct Recovery = 79% Analysis Date = 12/29/14 Pct Recovery = 79% Analysis Date = 12/19/14 Pct Recovery = 79% Analysis Date = 12/19/14 Pct Recovery = 79% Analysis Date = 12/09/14 Pct Recovery = 79% Analysis Date = 12/09/14 Pct Recovery = 79% Analysis Date = 11/29/14 Pct Recovery = 79% Analysis Date = 11/29/14 Pct Recovery = 79% Analysis Date = 11/19/14 Pct Recovery = 79% Analysis Date = 11/19/14 Pct Recovery = 79% Analysis Date = 11/09/14 Pct Recovery = 79% Analysis Date = 11/09/14 Pct Recovery = 79% Analysis Date = 10/31/14 Pct Recovery = 79% Analysis Date = 10/31/14 Pct Recovery = 79% Analysis Date = 10/21/14 Pct Recovery = 79% Analysis Date = 10/21/14 Pct Recovery = 79% Analysis Date = 10/11/14 Pct Recovery = 79% Analysis Date = 10/11/14 Pct Recovery = 79% Analysis Date = 10/01/14 Pct Recovery = 79% Analysis Date = 10/01/14 Pct Recovery = 79% Analysis Date = 09/21/14 Pct Recovery = 79% Analysis Date = 09/21/14 Pct Recovery = 79% Analysis Date = 09/11/14 Pct Recovery = 79% Analysis Date = 09/11/14 Pct Recovery = 79% Analysis Date = 09/01/14 Pct Recovery = 79% Analysis Date = 09/01/14 Pct Recovery = 79% Analysis Date = 08/22/14 Pct Recovery = 79% Analysis Date = 08/22/14 Pct Recovery = 79% Analysis Date = 08/12/14 Pct Recovery = 79% Analysis Date = 08/12/14 Pct Recovery = 79% Analysis Date = 08/02/14 Pct Recovery = 79% Analysis Date = 08/02/14 Pct Recovery = 79% Analysis Date = 07/23/14 Pct Recovery = 79% Analysis Date = 07/23/14 Pct Recovery = 79% Analysis Date = 07/14/14 Pct Recovery = 79% Analysis Date = 07/14/14 Pct Recovery = 79% Analysis Date = 07/04/14 Pct Recovery = 79% Analysis Date = 07/04/14 Pct Recovery = 79% Analysis Date = 06/24/14 Pct Recovery = 79% Analysis Date = 06/24/14 Pct Recovery = 79% Analysis Date = 06/14/14 Pct Recovery = 79% Analysis Date = 06/14/14 Pct Recovery = 79% Analysis Date = 06/04/14 Pct Recovery = 79% Analysis Date = 06/04/14 Pct Recovery = 79% Analysis Date = 05/25/14 Pct Recovery = 79% Analysis Date = 05/25/14 Pct Recovery = 79% Analysis Date = 05/15/14 Pct Recovery = 78% Analysis Date = 05/15/14 Pct Recovery = 78% Analysis Date = 05/05/14 Pct Recovery = 78% Analysis Date = 05/05/14 Pct Recovery = 78% Analysis Date = 04/25/14 Pct Recovery = 78% Analysis Date = 04/25/14 Pct Recovery = 78% Analysis Date = 04/15/14 Pct Recovery = 78% Analysis Date = 04/15/14 Pct Recovery = 78% Analysis Date = 04/05/14 Pct Recovery = 78% Analysis Date = 04/05/14 Pct Recovery = 78% Analysis Date = 03/27/14 Pct Recovery = 78% Analysis Date = 03/27/14 Pct Recovery = 78% Analysis Date = 03/17/14 Pct Recovery = 78% Analysis Date = 03/17/14 Pct Recovery = 78% Analysis Date = 03/07/14 Pct Recovery = 78% Analysis Date = 03/07/14 Pct Recovery = 78% Analysis Date = 02/25/14 Pct Recovery = 78% Analysis Date = 02/25/14 Pct Recovery = 78% Analysis Date = 02/15/14 Pct Recovery = 78% Analysis Date = 02/15/14 Pct Recovery = 78% Analysis Date = 02/05/14 Pct Recovery = 78% Analysis Date = 02/05/14 Pct Recovery = 78% Analysis Date = 01/26/14 Pct Recovery = 78% Analysis Date = 01/26/14 Pct Recovery = 78% Analysis Date = 01/16/14 Pct Recovery = 78% Analysis Date = 01/16/14 Pct Recovery = 78% Analysis Date = 01/06/14 Pct Recovery = 78% Analysis Date = 01/06/14 Pct Recovery = 78% Analysis Date = 12/27/13 Pct Recovery = 78% Analysis Date = 12/27/13 Pct Recovery = 78% Analysis Date = 12/17/13 Pct Recovery = 78% Analysis Date = 12/17/13 Pct Recovery = 78% Analysis Date = 12/08/13 Pct Recovery = 78% Analysis Date = 12/08/13 Pct Recovery = 78% Analysis Date = 11/28/13 Pct Recovery = 77% Analysis Date = 11/28/13 Pct Recovery = 77% Analysis Date = 11/18/13 Pct Recovery = 77% Analysis Date = 11/18/13 Pct Recovery = 77% Analysis Date = 11/08/13 Pct Recovery = 77% Analysis Date = 11/08/13 Pct Recovery = 77% Analysis Date = 10/29/13 Pct Recovery = 77% Analysis Date = 10/29/13 Pct Recovery = 77% Analysis Date = 10/19/13 Pct Recovery = 77% Analysis Date = 10/19/13 Pct Recovery = 77% Analysis Date = 10/09/13 Pct Recovery = 77% Analysis Date = 10/09/13 Pct Recovery = 77% Analysis Date = 09/29/13 Pct Recovery = 77% Analysis Date = 09/29/13 Pct Recovery = 77% Analysis Date = 09/19/13 Pct Recovery = 77% Analysis Date = 09/19/13 Pct Recovery = 77% Analysis Date = 09/09/13 Pct Recovery = 77% Analysis Date = 09/09/13 Pct Recovery = 77% Analysis Date = 08/30/13 Pct Recovery = 77% Analysis Date = 08/30/13 Pct Recovery = 77% Analysis Date = 08/21/13 Pct Recovery = 77% Analysis Date = 08/21/13 Pct Recovery = 77% Analysis Date = 08/11/13 Pct Recovery = 77% Analysis Date = 08/11/13 Pct Recovery = 77% Analysis Date = 08/01/13 Pct Recovery = 77% Analysis Date = 08/01/13 Pct Recovery = 77% Analysis Date = 07/22/13 Pct Recovery = 77% Analysis Date = 07/22/13 Pct Recovery = 77% Analysis Date = 07/12/13 Pct Recovery = 77% Analysis Date = 07/12/13 Pct Recovery = 77% Analysis Date = 07/02/13 Pct Recovery = 77% Analysis Date = 07/02/13 Pct Recovery = 77% Analysis Date = 06/22/13 Pct Recovery = 77% Analysis Date = 06/22/13 Pct Recovery = 77% Analysis Date = 06/12/13 Pct Recovery = 76% Analysis Date = 06/12/13 Pct Recovery = 76% Analysis Date = 06/02/13 Pct Recovery = 76% Analysis Date = 06/02/13 Pct Recovery = 76% Analysis Date = 05/23/13 Pct Recovery = 76% Analysis Date = 05/23/13 Pct Recovery = 76% Analysis Date = 05/13/13 Pct Recovery = 76% Analysis Date = 05/13/13 Pct Recovery = 76% Analysis Date = 05/04/13 Pct Recovery = 76% Analysis Date = 05/04/13 Pct Recovery = 76% Analysis Date = 04/24/13 Pct Recovery = 76% Analysis Date = 04/24/13 Pct Recovery = 76% Analysis Date = 04/14/13 Pct Recovery = 76% Analysis Date = 04/14/13 Pct Recovery = 76% Analysis Date = 04/04/13 Pct Recovery = 76% Analysis Date = 04/04/13 Pct Recovery = 76% Analysis Date = 03/25/13 Pct Recovery = 76% Analysis Date = 03/25/13 Pct Recovery = 76% Analysis Date = 03/15/13 Pct Recovery = 76% Analysis Date = 03/15/13 Pct Recovery = 76% Analysis Date = 03/05/13 Pct Recovery = 76% Analysis Date = 03/05/13 Pct Recovery = 76% Analysis Date = 02/23/13 Pct Recovery = 76% Analysis Date = 02/23/13 Pct Recovery = 76% Analysis Date = 02/13/13 Pct Recovery = 76% Analysis Date = 02/13/13 Pct Recovery = 76% Analysis Date = 02/03/13 Pct Recovery = 76% Analysis Date = 02/03/13 Pct Recovery = 76% Analysis Date = 01/24/13 Pct Recovery = 76% Analysis Date = 01/24/13 Pct Recovery = 76% Analysis Date = 01/15/13 Pct Recovery = 76% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
METRIBUZIN

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 75 78% 16% 77% 14%
Total 75 78% 16% 77% 14%

Sample Statistics
METRIBUZIN

Characteristic N % % Basis
Plotted 75 100% Spiked
Estimated Values 1 1% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 75 .  
False Negatives 0 0% 0 out of 75
Not Spiked 59 .  
False Positives 0 0% 0 out of 59

OBSP Determination:
MOLINATE
METHOD: 2033 , TESTIDCODE: 82671GCM35

Laboratory ID = 20130250061 Lab Value = 0.268 Expected Conc. = 0.3 Report level label = 0.008 Pct Recovery = 89% Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl SpecificMix = A088380 Laboratory ID = 20140230082 Lab Value = 0.134 Expected Conc. = 0.15 Report level label = 0.008 Pct Recovery = 89% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl SpecificMix = A093651 Laboratory ID = 20132420001 Lab Value = 0.140 Expected Conc. = 0.15 Report level label = 0.008 Pct Recovery = 93% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl SpecificMix = A093651 Laboratory ID = 20130810108 Lab Value = 0.134 Expected Conc. = 0.15 Report level label = 0.008 Pct Recovery = 89% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl SpecificMix = T1120530013 Laboratory ID = 20123560092 Lab Value = 0.126 Expected Conc. = 0.15 Report level label = 0.008 Pct Recovery = 84% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = T1120530013 Laboratory ID = 20140100085 Lab Value = 0.102 Expected Conc. = 0.1 Report level label = 0.008 Pct Recovery = 102% Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl SpecificMix = T1130514013 Laboratory ID = 20132490342 Lab Value = 0.096 Expected Conc. = 0.1 Report level label = 0.008 Pct Recovery = 96% Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl SpecificMix = T1130514013 Laboratory ID = 20140860102 Lab Value = 0.052 Expected Conc. = 0.06 Report level label = 0.008 Pct Recovery = 86% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl SpecificMix = A093651 Laboratory ID = 20133400002 Lab Value = 0.060 Expected Conc. = 0.06 Report level label = 0.008 Pct Recovery = 100% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = A093651 Laboratory ID = 20132910008 Lab Value = 0.060 Expected Conc. = 0.06 Report level label = 0.008 Pct Recovery = 99% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = A093651 Laboratory ID = 20131920149 Lab Value = 0.060 Expected Conc. = 0.06 Report level label = 0.008 Pct Recovery = 100% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl SpecificMix = A093651 Laboratory ID = 20131230084 Lab Value = 0.063 Expected Conc. = 0.06 Report level label = 0.008 Pct Recovery = 106% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl SpecificMix = A088380 Laboratory ID = 20130650005 Lab Value = 0.054 Expected Conc. = 0.06 Report level label = 0.008 Pct Recovery = 91% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl SpecificMix = A088380 Laboratory ID = 20130390105 Lab Value = 0.049 Expected Conc. = 0.06 Report level label = 0.008 Pct Recovery = 82% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl SpecificMix = T1120530013 Laboratory ID = 20163370001 Lab Value = 0.057 Expected Conc. = 0.0503 Report level label = 0.008 Pct Recovery = 112% Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl SpecificMix = LC20138V Laboratory ID = 20162860079 Lab Value = 0.057 Expected Conc. = 0.05 Report level label = 0.008 Pct Recovery = 115% Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl SpecificMix = 5054800 Laboratory ID = 20161880109 Lab Value = 0.061 Expected Conc. = 0.05 Report level label = 0.008 Pct Recovery = 123% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl SpecificMix = 5054800 Laboratory ID = 20140370077 Lab Value = 0.044 Expected Conc. = 0.05 Report level label = 0.008 Pct Recovery = 87% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl SpecificMix = T1130514013 Laboratory ID = 20132690010 Lab Value = 0.061 Expected Conc. = 0.05 Report level label = 0.008 Pct Recovery = 122% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl SpecificMix = T1130514013 Laboratory ID = 20131370001 Lab Value = 0.055 Expected Conc. = 0.05 Report level label = 0.008 Pct Recovery = 109% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl SpecificMix = 1473000 Laboratory ID = 20152750006 Lab Value = 0.020 Expected Conc. = 0.048 Report level label = 0.008 Pct Recovery = 41% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl SpecificMix = EN150514012 Laboratory ID = 20152460215 Lab Value = 0.046 Expected Conc. = 0.048 Report level label = 0.008 Pct Recovery = 96% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl SpecificMix = EN150514012 Laboratory ID = 20171720140 Lab Value = 0.046 Expected Conc. = 0.0402 Report level label = 0.008 Pct Recovery = 114% Analysis Date = 08/31/17 SpikeMix = Supelco LC20138V: 80 µl & Phenova B20160331: 80 µl SpecificMix = LC20138V Laboratory ID = 20170740063 Lab Value = 0.048 Expected Conc. = 0.0402 Report level label = 0.008 Pct Recovery = 119% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl SpecificMix = LC20138V Laboratory ID = 20161470001 Lab Value = 0.042 Expected Conc. = 0.0402 Report level label = 0.008 Pct Recovery = 103% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl SpecificMix = LC20138V Laboratory ID = 20171380001 Lab Value = 0.035 Expected Conc. = 0.04 Report level label = 0.008 Pct Recovery = 88% Analysis Date = 06/07/17 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 5054800 Laboratory ID = 20170960001 Lab Value = 0.046 Expected Conc. = 0.04 Report level label = 0.008 Pct Recovery = 115% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl SpecificMix = 5054800 Laboratory ID = 20161740258 Lab Value = 0.034 Expected Conc. = 0.04 Report level label = 0.008 Pct Recovery = 84% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 5054800 Laboratory ID = 20150720069 Lab Value = 0.031 Expected Conc. = 0.0318 Report level label = 0.008 Pct Recovery = 98% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 03DD006 Laboratory ID = 20143110108 Lab Value = 0.024 Expected Conc. = 0.0318 Report level label = 0.008 Pct Recovery = 77% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 03DD006 Laboratory ID = 20142960086 Lab Value = 0.027 Expected Conc. = 0.0318 Report level label = 0.008 Pct Recovery = 86% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 03DD006 Laboratory ID = 20142720002 Lab Value = 0.028 Expected Conc. = 0.0318 Report level label = 0.008 Pct Recovery = 87% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl SpecificMix = LC06435 Laboratory ID = 20142530087 Lab Value = 0.028 Expected Conc. = 0.0318 Report level label = 0.008 Pct Recovery = 87% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl SpecificMix = LC06435 Laboratory ID = 20142270001 Lab Value = 0.025 Expected Conc. = 0.0318 Report level label = 0.008 Pct Recovery = 79% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl SpecificMix = 03DD006 Laboratory ID = 20141570088 Lab Value = 0.034 Expected Conc. = 0.0318 Report level label = 0.008 Pct Recovery = 108% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl SpecificMix = LC06435 Laboratory ID = 20141220025 Lab Value = 0.038 Expected Conc. = 0.0318 Report level label = 0.008 Pct Recovery = 118% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl SpecificMix = LC06435 Laboratory ID = 20172560101 Lab Value = 0.027 Expected Conc. = 0.0271 Report level label = 0.008 Pct Recovery = 98% Analysis Date = 12/22/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6567600: 50 µl SpecificMix = EN170808006 Laboratory ID = 20172370001 Lab Value = 0.029 Expected Conc. = 0.0271 Report level label = 0.008 Pct Recovery = 106% Analysis Date = 11/18/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6537100: 50 µl SpecificMix = EN170808006 Laboratory ID = 20172230001 Lab Value = 0.032 Expected Conc. = 0.025 Report level label = 0.008 Pct Recovery = 128% Analysis Date = 10/19/17 SpikeMix = ChemService 6472100: 50 µl & Abs 071717Pest: 50 µl SpecificMix = 6472100 Laboratory ID = 20153440001 Lab Value = 0.021 Expected Conc. = 0.024 Report level label = 0.008 Pct Recovery = 87% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = EN150514012 Laboratory ID = 20152330039 Lab Value = 0.018 Expected Conc. = 0.024 Report level label = 0.008 Pct Recovery = 73% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl SpecificMix = 041415 Laboratory ID = 20151900132 Lab Value = 0.018 Expected Conc. = 0.024 Report level label = 0.008 Pct Recovery = 73% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl SpecificMix = 041415 Laboratory ID = 20151270112 Lab Value = 0.026 Expected Conc. = 0.024 Report level label = 0.008 Pct Recovery = 109% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl SpecificMix = 041415 Laboratory ID = 20171510080 Lab Value = 0.024 Expected Conc. = 0.0201 Report level label = 0.008 Pct Recovery = 117% Analysis Date = 06/09/17 SpikeMix = Supelco LC20138V: 40 µl & Crescent 03FF076: 40 µl SpecificMix = LC20138V Laboratory ID = 20162520001 Lab Value = 0.027 Expected Conc. = 0.0201 Report level label = 0.008 Pct Recovery = 135% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl SpecificMix = LC20138V Laboratory ID = 20162660005 Lab Value = 0.024 Expected Conc. = 0.0201 Report level label = 0.008 Pct Recovery = 117% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl SpecificMix = LC20138V Laboratory ID = 20162020124 Lab Value = 0.021 Expected Conc. = 0.0201 Report level label = 0.008 Pct Recovery = 105% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl SpecificMix = LC20138V Laboratory ID = 20171940002 Lab Value = 0.024 Expected Conc. = 0.02 Report level label = 0.008 Pct Recovery = 121% Analysis Date = 11/10/17 SpikeMix = ChemService 5054800: 40 µl & NSI 041816: 40 µl SpecificMix = 5054800 Laboratory ID = 20170460061 Lab Value = 0.024 Expected Conc. = 0.02 Report level label = 0.008 Pct Recovery = 122% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl SpecificMix = 5054800 Laboratory ID = 20163560019 Lab Value = 0.023 Expected Conc. = 0.02 Report level label = 0.008 Pct Recovery = 113% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl SpecificMix = 5054800 Laboratory ID = 20162150213 Lab Value = 0.020 Expected Conc. = 0.02 Report level label = 0.008 Pct Recovery = 98% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl SpecificMix = 5054800 Laboratory ID = 20140730138 Lab Value = 0.022 Expected Conc. = 0.02 Report level label = 0.008 Pct Recovery = 110% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 1473000 Laboratory ID = 20133470008 Lab Value = 0.021 Expected Conc. = 0.02 Report level label = 0.008 Pct Recovery = 103% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl SpecificMix = 1473000 Laboratory ID = 20133310030 Lab Value = 0.021 Expected Conc. = 0.02 Report level label = 0.008 Pct Recovery = 105% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl SpecificMix = 1473000 Laboratory ID = 20133050050 Lab Value = 0.023 Expected Conc. = 0.02 Report level label = 0.008 Pct Recovery = 113% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl SpecificMix = T1130514013 Laboratory ID = 20132280016 Lab Value = 0.024 Expected Conc. = 0.02 Report level label = 0.008 Pct Recovery = 118% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl SpecificMix = T1130514013 Laboratory ID = 20131790009 Lab Value = 0.022 Expected Conc. = 0.02 Report level label = 0.008 Pct Recovery = 108% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl SpecificMix = 1473000 Laboratory ID = 20131650073 Lab Value = 0.024 Expected Conc. = 0.02 Report level label = 0.008 Pct Recovery = 118% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl SpecificMix = 1473000 Laboratory ID = 20150150115 Lab Value = 0.013 Expected Conc. = 0.0159 Report level label = 0.008 Pct Recovery = 82% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl SpecificMix = LC06435 Laboratory ID = 20142200164 Lab Value = 0.015 Expected Conc. = 0.0159 Report level label = 0.008 Pct Recovery = 92% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 03DD006 Laboratory ID = 20141910243 Lab Value = 0.014 Expected Conc. = 0.0159 Report level label = 0.008 Pct Recovery = 85% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = LC06435 Laboratory ID = 20141840097 Lab Value = 0.014 Expected Conc. = 0.0159 Report level label = 0.008 Pct Recovery = 90% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl SpecificMix = LC06435 Laboratory ID = 20141640076 Lab Value = 0.014 Expected Conc. = 0.0159 Report level label = 0.008 Pct Recovery = 89% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = 03DD006 Laboratory ID = 20141420140 Lab Value = 0.015 Expected Conc. = 0.0159 Report level label = 0.008 Pct Recovery = 93% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 03DD006 Laboratory ID = 20141080004 Lab Value = 0.015 Expected Conc. = 0.0159 Report level label = 0.008 Pct Recovery = 92% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl SpecificMix = 03DD006 Laboratory ID = 20173120093 Lab Value = 0.019 Expected Conc. = 0.015 Report level label = 0.008 Pct Recovery = 127% Analysis Date = 03/10/18 SpikeMix = ChemService 6472100: 30 µl & ChemService 6537100: 30 µl SpecificMix = 6472100 Laboratory ID = 20161050143 Lab Value = 0.013 Expected Conc. = 0.012 Report level label = 0.008 Pct Recovery = 108% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 041415 Laboratory ID = 20160070059 Lab Value = 0.013 Expected Conc. = 0.012 Report level label = 0.008 Pct Recovery = 108% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = EN150514012 Laboratory ID = 20153160001 Lab Value = 0.013 Expected Conc. = 0.012 Report level label = 0.008 Pct Recovery = 107% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = EN150514012 Laboratory ID = 20152950078 Lab Value = 0.008 Expected Conc. = 0.012 Report level label = 0.008 Pct Recovery = 65% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 041415 Laboratory ID = 20152040177 Lab Value = 0.011 Expected Conc. = 0.012 Report level label = 0.008 Pct Recovery = 94% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl SpecificMix = 041415 Laboratory ID = 20151760208 Lab Value = 0.009 Expected Conc. = 0.012 Report level label = 0.008 Pct Recovery = 73% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl SpecificMix = EN150514012 Laboratory ID = 20151480170 Lab Value = 0.012 Expected Conc. = 0.012 Report level label = 0.008 Pct Recovery = 101% Analysis Date = 06/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150514012 Laboratory ID = 20151210037 Lab Value = 0.014 Expected Conc. = 0.012 Report level label = 0.008 Pct Recovery = 113% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 041415 Analysis Date = 03/10/18 Pct Recovery = 123% Analysis Date = 02/28/18 Pct Recovery = 123% Analysis Date = 02/28/18 Pct Recovery = 123% Analysis Date = 02/19/18 Pct Recovery = 123% Analysis Date = 02/19/18 Pct Recovery = 123% Analysis Date = 02/09/18 Pct Recovery = 122% Analysis Date = 02/09/18 Pct Recovery = 122% Analysis Date = 01/31/18 Pct Recovery = 122% Analysis Date = 01/31/18 Pct Recovery = 122% Analysis Date = 01/22/18 Pct Recovery = 122% Analysis Date = 01/22/18 Pct Recovery = 122% Analysis Date = 01/12/18 Pct Recovery = 121% Analysis Date = 01/12/18 Pct Recovery = 121% Analysis Date = 01/03/18 Pct Recovery = 121% Analysis Date = 01/03/18 Pct Recovery = 121% Analysis Date = 12/24/17 Pct Recovery = 121% Analysis Date = 12/24/17 Pct Recovery = 121% Analysis Date = 12/15/17 Pct Recovery = 120% Analysis Date = 12/15/17 Pct Recovery = 120% Analysis Date = 12/06/17 Pct Recovery = 120% Analysis Date = 12/06/17 Pct Recovery = 120% Analysis Date = 11/26/17 Pct Recovery = 120% Analysis Date = 11/26/17 Pct Recovery = 120% Analysis Date = 11/17/17 Pct Recovery = 119% Analysis Date = 11/17/17 Pct Recovery = 119% Analysis Date = 11/07/17 Pct Recovery = 119% Analysis Date = 11/07/17 Pct Recovery = 119% Analysis Date = 10/29/17 Pct Recovery = 119% Analysis Date = 10/29/17 Pct Recovery = 119% Analysis Date = 10/20/17 Pct Recovery = 118% Analysis Date = 10/20/17 Pct Recovery = 118% Analysis Date = 10/10/17 Pct Recovery = 118% Analysis Date = 10/10/17 Pct Recovery = 118% Analysis Date = 10/01/17 Pct Recovery = 117% Analysis Date = 10/01/17 Pct Recovery = 117% Analysis Date = 09/21/17 Pct Recovery = 117% Analysis Date = 09/21/17 Pct Recovery = 117% Analysis Date = 09/12/17 Pct Recovery = 117% Analysis Date = 09/12/17 Pct Recovery = 117% Analysis Date = 09/03/17 Pct Recovery = 116% Analysis Date = 09/03/17 Pct Recovery = 116% Analysis Date = 08/24/17 Pct Recovery = 116% Analysis Date = 08/24/17 Pct Recovery = 116% Analysis Date = 08/15/17 Pct Recovery = 116% Analysis Date = 08/15/17 Pct Recovery = 116% Analysis Date = 08/05/17 Pct Recovery = 115% Analysis Date = 08/05/17 Pct Recovery = 115% Analysis Date = 07/27/17 Pct Recovery = 115% Analysis Date = 07/27/17 Pct Recovery = 115% Analysis Date = 07/18/17 Pct Recovery = 115% Analysis Date = 07/18/17 Pct Recovery = 115% Analysis Date = 07/08/17 Pct Recovery = 114% Analysis Date = 07/08/17 Pct Recovery = 114% Analysis Date = 06/29/17 Pct Recovery = 114% Analysis Date = 06/29/17 Pct Recovery = 114% Analysis Date = 06/19/17 Pct Recovery = 114% Analysis Date = 06/19/17 Pct Recovery = 114% Analysis Date = 06/10/17 Pct Recovery = 113% Analysis Date = 06/10/17 Pct Recovery = 113% Analysis Date = 06/01/17 Pct Recovery = 113% Analysis Date = 06/01/17 Pct Recovery = 113% Analysis Date = 05/22/17 Pct Recovery = 112% Analysis Date = 05/22/17 Pct Recovery = 112% Analysis Date = 05/13/17 Pct Recovery = 112% Analysis Date = 05/13/17 Pct Recovery = 112% Analysis Date = 05/03/17 Pct Recovery = 112% Analysis Date = 05/03/17 Pct Recovery = 112% Analysis Date = 04/24/17 Pct Recovery = 111% Analysis Date = 04/24/17 Pct Recovery = 111% Analysis Date = 04/15/17 Pct Recovery = 111% Analysis Date = 04/15/17 Pct Recovery = 111% Analysis Date = 04/05/17 Pct Recovery = 111% Analysis Date = 04/05/17 Pct Recovery = 111% Analysis Date = 03/27/17 Pct Recovery = 110% Analysis Date = 03/27/17 Pct Recovery = 110% Analysis Date = 03/17/17 Pct Recovery = 110% Analysis Date = 03/17/17 Pct Recovery = 110% Analysis Date = 03/08/17 Pct Recovery = 110% Analysis Date = 03/08/17 Pct Recovery = 110% Analysis Date = 02/27/17 Pct Recovery = 109% Analysis Date = 02/27/17 Pct Recovery = 109% Analysis Date = 02/17/17 Pct Recovery = 109% Analysis Date = 02/17/17 Pct Recovery = 109% Analysis Date = 02/08/17 Pct Recovery = 109% Analysis Date = 02/08/17 Pct Recovery = 109% Analysis Date = 01/29/17 Pct Recovery = 108% Analysis Date = 01/29/17 Pct Recovery = 108% Analysis Date = 01/20/17 Pct Recovery = 108% Analysis Date = 01/20/17 Pct Recovery = 108% Analysis Date = 01/11/17 Pct Recovery = 107% Analysis Date = 01/11/17 Pct Recovery = 107% Analysis Date = 01/01/17 Pct Recovery = 107% Analysis Date = 01/01/17 Pct Recovery = 107% Analysis Date = 12/23/16 Pct Recovery = 107% Analysis Date = 12/23/16 Pct Recovery = 107% Analysis Date = 12/13/16 Pct Recovery = 106% Analysis Date = 12/13/16 Pct Recovery = 106% Analysis Date = 12/04/16 Pct Recovery = 106% Analysis Date = 12/04/16 Pct Recovery = 106% Analysis Date = 11/25/16 Pct Recovery = 106% Analysis Date = 11/25/16 Pct Recovery = 106% Analysis Date = 11/15/16 Pct Recovery = 105% Analysis Date = 11/15/16 Pct Recovery = 105% Analysis Date = 11/06/16 Pct Recovery = 105% Analysis Date = 11/06/16 Pct Recovery = 105% Analysis Date = 10/27/16 Pct Recovery = 105% Analysis Date = 10/27/16 Pct Recovery = 105% Analysis Date = 10/18/16 Pct Recovery = 104% Analysis Date = 10/18/16 Pct Recovery = 104% Analysis Date = 10/09/16 Pct Recovery = 104% Analysis Date = 10/09/16 Pct Recovery = 104% Analysis Date = 09/29/16 Pct Recovery = 104% Analysis Date = 09/29/16 Pct Recovery = 104% Analysis Date = 09/20/16 Pct Recovery = 103% Analysis Date = 09/20/16 Pct Recovery = 103% Analysis Date = 09/10/16 Pct Recovery = 103% Analysis Date = 09/10/16 Pct Recovery = 103% Analysis Date = 09/01/16 Pct Recovery = 103% Analysis Date = 09/01/16 Pct Recovery = 103% Analysis Date = 08/23/16 Pct Recovery = 102% Analysis Date = 08/23/16 Pct Recovery = 102% Analysis Date = 08/13/16 Pct Recovery = 102% Analysis Date = 08/13/16 Pct Recovery = 102% Analysis Date = 08/04/16 Pct Recovery = 102% Analysis Date = 08/04/16 Pct Recovery = 102% Analysis Date = 07/25/16 Pct Recovery = 101% Analysis Date = 07/25/16 Pct Recovery = 101% Analysis Date = 07/16/16 Pct Recovery = 101% Analysis Date = 07/16/16 Pct Recovery = 101% Analysis Date = 07/07/16 Pct Recovery = 101% Analysis Date = 07/07/16 Pct Recovery = 101% Analysis Date = 06/27/16 Pct Recovery = 100% Analysis Date = 06/27/16 Pct Recovery = 100% Analysis Date = 06/18/16 Pct Recovery = 100% Analysis Date = 06/18/16 Pct Recovery = 100% Analysis Date = 06/08/16 Pct Recovery = 100% Analysis Date = 06/08/16 Pct Recovery = 100% Analysis Date = 05/30/16 Pct Recovery = 99% Analysis Date = 05/30/16 Pct Recovery = 99% Analysis Date = 05/21/16 Pct Recovery = 99% Analysis Date = 05/21/16 Pct Recovery = 99% Analysis Date = 05/11/16 Pct Recovery = 99% Analysis Date = 05/11/16 Pct Recovery = 99% Analysis Date = 05/02/16 Pct Recovery = 98% Analysis Date = 05/02/16 Pct Recovery = 98% Analysis Date = 04/22/16 Pct Recovery = 98% Analysis Date = 04/22/16 Pct Recovery = 98% Analysis Date = 04/13/16 Pct Recovery = 98% Analysis Date = 04/13/16 Pct Recovery = 98% Analysis Date = 04/04/16 Pct Recovery = 97% Analysis Date = 04/04/16 Pct Recovery = 97% Analysis Date = 03/25/16 Pct Recovery = 97% Analysis Date = 03/25/16 Pct Recovery = 97% Analysis Date = 03/16/16 Pct Recovery = 97% Analysis Date = 03/16/16 Pct Recovery = 97% Analysis Date = 03/06/16 Pct Recovery = 96% Analysis Date = 03/06/16 Pct Recovery = 96% Analysis Date = 02/26/16 Pct Recovery = 96% Analysis Date = 02/26/16 Pct Recovery = 96% Analysis Date = 02/17/16 Pct Recovery = 95% Analysis Date = 02/17/16 Pct Recovery = 95% Analysis Date = 02/07/16 Pct Recovery = 95% Analysis Date = 02/07/16 Pct Recovery = 95% Analysis Date = 01/29/16 Pct Recovery = 95% Analysis Date = 01/29/16 Pct Recovery = 95% Analysis Date = 01/19/16 Pct Recovery = 95% Analysis Date = 01/19/16 Pct Recovery = 95% Analysis Date = 01/10/16 Pct Recovery = 94% Analysis Date = 01/10/16 Pct Recovery = 94% Analysis Date = 01/01/16 Pct Recovery = 94% Analysis Date = 01/01/16 Pct Recovery = 94% Analysis Date = 12/22/15 Pct Recovery = 94% Analysis Date = 12/22/15 Pct Recovery = 94% Analysis Date = 12/13/15 Pct Recovery = 93% Analysis Date = 12/13/15 Pct Recovery = 93% Analysis Date = 12/03/15 Pct Recovery = 93% Analysis Date = 12/03/15 Pct Recovery = 93% Analysis Date = 11/24/15 Pct Recovery = 93% Analysis Date = 11/24/15 Pct Recovery = 93% Analysis Date = 11/15/15 Pct Recovery = 92% Analysis Date = 11/15/15 Pct Recovery = 92% Analysis Date = 11/05/15 Pct Recovery = 92% Analysis Date = 11/05/15 Pct Recovery = 92% Analysis Date = 10/27/15 Pct Recovery = 92% Analysis Date = 10/27/15 Pct Recovery = 92% Analysis Date = 10/17/15 Pct Recovery = 91% Analysis Date = 10/17/15 Pct Recovery = 91% Analysis Date = 10/08/15 Pct Recovery = 91% Analysis Date = 10/08/15 Pct Recovery = 91% Analysis Date = 09/29/15 Pct Recovery = 91% Analysis Date = 09/29/15 Pct Recovery = 91% Analysis Date = 09/19/15 Pct Recovery = 91% Analysis Date = 09/19/15 Pct Recovery = 91% Analysis Date = 09/10/15 Pct Recovery = 90% Analysis Date = 09/10/15 Pct Recovery = 90% Analysis Date = 08/31/15 Pct Recovery = 90% Analysis Date = 08/31/15 Pct Recovery = 90% Analysis Date = 08/22/15 Pct Recovery = 90% Analysis Date = 08/22/15 Pct Recovery = 90% Analysis Date = 08/13/15 Pct Recovery = 90% Analysis Date = 08/13/15 Pct Recovery = 90% Analysis Date = 08/03/15 Pct Recovery = 90% Analysis Date = 08/03/15 Pct Recovery = 90% Analysis Date = 07/25/15 Pct Recovery = 90% Analysis Date = 07/25/15 Pct Recovery = 90% Analysis Date = 07/15/15 Pct Recovery = 90% Analysis Date = 07/15/15 Pct Recovery = 90% Analysis Date = 07/06/15 Pct Recovery = 90% Analysis Date = 07/06/15 Pct Recovery = 90% Analysis Date = 06/27/15 Pct Recovery = 90% Analysis Date = 06/27/15 Pct Recovery = 90% Analysis Date = 06/17/15 Pct Recovery = 89% Analysis Date = 06/17/15 Pct Recovery = 89% Analysis Date = 06/08/15 Pct Recovery = 89% Analysis Date = 06/08/15 Pct Recovery = 89% Analysis Date = 05/29/15 Pct Recovery = 89% Analysis Date = 05/29/15 Pct Recovery = 89% Analysis Date = 05/20/15 Pct Recovery = 90% Analysis Date = 05/20/15 Pct Recovery = 90% Analysis Date = 05/11/15 Pct Recovery = 90% Analysis Date = 05/11/15 Pct Recovery = 90% Analysis Date = 05/01/15 Pct Recovery = 90% Analysis Date = 05/01/15 Pct Recovery = 90% Analysis Date = 04/22/15 Pct Recovery = 90% Analysis Date = 04/22/15 Pct Recovery = 90% Analysis Date = 04/12/15 Pct Recovery = 90% Analysis Date = 04/12/15 Pct Recovery = 90% Analysis Date = 04/03/15 Pct Recovery = 90% Analysis Date = 04/03/15 Pct Recovery = 90% Analysis Date = 03/25/15 Pct Recovery = 90% Analysis Date = 03/25/15 Pct Recovery = 90% Analysis Date = 03/15/15 Pct Recovery = 90% Analysis Date = 03/15/15 Pct Recovery = 90% Analysis Date = 03/06/15 Pct Recovery = 90% Analysis Date = 03/06/15 Pct Recovery = 90% Analysis Date = 02/24/15 Pct Recovery = 91% Analysis Date = 02/24/15 Pct Recovery = 91% Analysis Date = 02/15/15 Pct Recovery = 91% Analysis Date = 02/15/15 Pct Recovery = 91% Analysis Date = 02/06/15 Pct Recovery = 91% Analysis Date = 02/06/15 Pct Recovery = 91% Analysis Date = 01/27/15 Pct Recovery = 91% Analysis Date = 01/27/15 Pct Recovery = 91% Analysis Date = 01/18/15 Pct Recovery = 91% Analysis Date = 01/18/15 Pct Recovery = 91% Analysis Date = 01/08/15 Pct Recovery = 91% Analysis Date = 01/08/15 Pct Recovery = 91% Analysis Date = 12/30/14 Pct Recovery = 91% Analysis Date = 12/30/14 Pct Recovery = 91% Analysis Date = 12/21/14 Pct Recovery = 91% Analysis Date = 12/21/14 Pct Recovery = 91% Analysis Date = 12/11/14 Pct Recovery = 91% Analysis Date = 12/11/14 Pct Recovery = 91% Analysis Date = 12/02/14 Pct Recovery = 92% Analysis Date = 12/02/14 Pct Recovery = 92% Analysis Date = 11/22/14 Pct Recovery = 92% Analysis Date = 11/22/14 Pct Recovery = 92% Analysis Date = 11/13/14 Pct Recovery = 92% Analysis Date = 11/13/14 Pct Recovery = 92% Analysis Date = 11/04/14 Pct Recovery = 92% Analysis Date = 11/04/14 Pct Recovery = 92% Analysis Date = 10/25/14 Pct Recovery = 92% Analysis Date = 10/25/14 Pct Recovery = 92% Analysis Date = 10/16/14 Pct Recovery = 92% Analysis Date = 10/16/14 Pct Recovery = 92% Analysis Date = 10/06/14 Pct Recovery = 93% Analysis Date = 10/06/14 Pct Recovery = 93% Analysis Date = 09/27/14 Pct Recovery = 93% Analysis Date = 09/27/14 Pct Recovery = 93% Analysis Date = 09/18/14 Pct Recovery = 93% Analysis Date = 09/18/14 Pct Recovery = 93% Analysis Date = 09/08/14 Pct Recovery = 93% Analysis Date = 09/08/14 Pct Recovery = 93% Analysis Date = 08/30/14 Pct Recovery = 94% Analysis Date = 08/30/14 Pct Recovery = 94% Analysis Date = 08/20/14 Pct Recovery = 94% Analysis Date = 08/20/14 Pct Recovery = 94% Analysis Date = 08/11/14 Pct Recovery = 94% Analysis Date = 08/11/14 Pct Recovery = 94% Analysis Date = 08/02/14 Pct Recovery = 94% Analysis Date = 08/02/14 Pct Recovery = 94% Analysis Date = 07/23/14 Pct Recovery = 94% Analysis Date = 07/23/14 Pct Recovery = 94% Analysis Date = 07/14/14 Pct Recovery = 94% Analysis Date = 07/14/14 Pct Recovery = 94% Analysis Date = 07/04/14 Pct Recovery = 94% Analysis Date = 07/04/14 Pct Recovery = 94% Analysis Date = 06/25/14 Pct Recovery = 94% Analysis Date = 06/25/14 Pct Recovery = 94% Analysis Date = 06/16/14 Pct Recovery = 95% Analysis Date = 06/16/14 Pct Recovery = 95% Analysis Date = 06/06/14 Pct Recovery = 95% Analysis Date = 06/06/14 Pct Recovery = 95% Analysis Date = 05/28/14 Pct Recovery = 95% Analysis Date = 05/28/14 Pct Recovery = 95% Analysis Date = 05/18/14 Pct Recovery = 95% Analysis Date = 05/18/14 Pct Recovery = 95% Analysis Date = 05/09/14 Pct Recovery = 96% Analysis Date = 05/09/14 Pct Recovery = 96% Analysis Date = 04/30/14 Pct Recovery = 96% Analysis Date = 04/30/14 Pct Recovery = 96% Analysis Date = 04/20/14 Pct Recovery = 96% Analysis Date = 04/20/14 Pct Recovery = 96% Analysis Date = 04/11/14 Pct Recovery = 96% Analysis Date = 04/11/14 Pct Recovery = 96% Analysis Date = 04/01/14 Pct Recovery = 96% Analysis Date = 04/01/14 Pct Recovery = 96% Analysis Date = 03/23/14 Pct Recovery = 97% Analysis Date = 03/23/14 Pct Recovery = 97% Analysis Date = 03/14/14 Pct Recovery = 97% Analysis Date = 03/14/14 Pct Recovery = 97% Analysis Date = 03/04/14 Pct Recovery = 97% Analysis Date = 03/04/14 Pct Recovery = 97% Analysis Date = 02/23/14 Pct Recovery = 97% Analysis Date = 02/23/14 Pct Recovery = 97% Analysis Date = 02/13/14 Pct Recovery = 97% Analysis Date = 02/13/14 Pct Recovery = 97% Analysis Date = 02/04/14 Pct Recovery = 98% Analysis Date = 02/04/14 Pct Recovery = 98% Analysis Date = 01/26/14 Pct Recovery = 98% Analysis Date = 01/26/14 Pct Recovery = 98% Analysis Date = 01/16/14 Pct Recovery = 98% Analysis Date = 01/16/14 Pct Recovery = 98% Analysis Date = 01/07/14 Pct Recovery = 98% Analysis Date = 01/07/14 Pct Recovery = 98% Analysis Date = 12/28/13 Pct Recovery = 98% Analysis Date = 12/28/13 Pct Recovery = 98% Analysis Date = 12/19/13 Pct Recovery = 98% Analysis Date = 12/19/13 Pct Recovery = 98% Analysis Date = 12/10/13 Pct Recovery = 98% Analysis Date = 12/10/13 Pct Recovery = 98% Analysis Date = 11/30/13 Pct Recovery = 98% Analysis Date = 11/30/13 Pct Recovery = 98% Analysis Date = 11/21/13 Pct Recovery = 98% Analysis Date = 11/21/13 Pct Recovery = 98% Analysis Date = 11/11/13 Pct Recovery = 99% Analysis Date = 11/11/13 Pct Recovery = 99% Analysis Date = 11/02/13 Pct Recovery = 99% Analysis Date = 11/02/13 Pct Recovery = 99% Analysis Date = 10/24/13 Pct Recovery = 99% Analysis Date = 10/24/13 Pct Recovery = 99% Analysis Date = 10/14/13 Pct Recovery = 99% Analysis Date = 10/14/13 Pct Recovery = 99% Analysis Date = 10/05/13 Pct Recovery = 99% Analysis Date = 10/05/13 Pct Recovery = 99% Analysis Date = 09/25/13 Pct Recovery = 99% Analysis Date = 09/25/13 Pct Recovery = 99% Analysis Date = 09/16/13 Pct Recovery = 99% Analysis Date = 09/16/13 Pct Recovery = 99% Analysis Date = 09/07/13 Pct Recovery = 99% Analysis Date = 09/07/13 Pct Recovery = 99% Analysis Date = 08/28/13 Pct Recovery = 99% Analysis Date = 08/28/13 Pct Recovery = 99% Analysis Date = 08/19/13 Pct Recovery = 99% Analysis Date = 08/19/13 Pct Recovery = 99% Analysis Date = 08/09/13 Pct Recovery = 99% Analysis Date = 08/09/13 Pct Recovery = 99% Analysis Date = 07/31/13 Pct Recovery = 99% Analysis Date = 07/31/13 Pct Recovery = 99% Analysis Date = 07/22/13 Pct Recovery = 99% Analysis Date = 07/22/13 Pct Recovery = 99% Analysis Date = 07/12/13 Pct Recovery = 99% Analysis Date = 07/12/13 Pct Recovery = 99% Analysis Date = 07/03/13 Pct Recovery = 99% Analysis Date = 07/03/13 Pct Recovery = 99% Analysis Date = 06/23/13 Pct Recovery = 99% Analysis Date = 06/23/13 Pct Recovery = 99% Analysis Date = 06/14/13 Pct Recovery = 100% Analysis Date = 06/14/13 Pct Recovery = 100% Analysis Date = 06/05/13 Pct Recovery = 100% Analysis Date = 06/05/13 Pct Recovery = 100% Analysis Date = 05/26/13 Pct Recovery = 100% Analysis Date = 05/26/13 Pct Recovery = 100% Analysis Date = 05/17/13 Pct Recovery = 100% Analysis Date = 05/17/13 Pct Recovery = 100% Analysis Date = 05/07/13 Pct Recovery = 100% Analysis Date = 05/07/13 Pct Recovery = 100% Analysis Date = 04/28/13 Pct Recovery = 100% Analysis Date = 04/28/13 Pct Recovery = 100% Analysis Date = 04/19/13 Pct Recovery = 100% Analysis Date = 04/19/13 Pct Recovery = 100% Analysis Date = 04/09/13 Pct Recovery = 100% Analysis Date = 04/09/13 Pct Recovery = 100% Analysis Date = 03/31/13 Pct Recovery = 100% Analysis Date = 03/31/13 Pct Recovery = 100% Analysis Date = 03/21/13 Pct Recovery = 100% Analysis Date = 03/21/13 Pct Recovery = 100% Analysis Date = 03/12/13 Pct Recovery = 100% Analysis Date = 03/12/13 Pct Recovery = 100% Analysis Date = 03/03/13 Pct Recovery = 100% Analysis Date = 03/03/13 Pct Recovery = 100% Analysis Date = 02/21/13 Pct Recovery = 100% Analysis Date = 02/21/13 Pct Recovery = 100% Analysis Date = 02/12/13 Pct Recovery = 100% Analysis Date = 02/12/13 Pct Recovery = 100% Analysis Date = 02/02/13 Pct Recovery = 100% Analysis Date = 02/02/13 Pct Recovery = 100% Analysis Date = 01/24/13 Pct Recovery = 100% Analysis Date = 01/24/13 Pct Recovery = 100% Analysis Date = 01/15/13 Pct Recovery = 100% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
MOLINATE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 74 100% 17% 100% 18%
Total 74 100% 17% 100% 18%

Sample Statistics
MOLINATE

Characteristic N % % Basis
Plotted 74 95% Spiked
Estimated Values 1 1% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 2 3% Spiked
Spiked 78 .  
False Negatives 2 3% 2 out of 78
Not Spiked 40 .  
False Positives 0 0% 0 out of 40

OBSP Determination:
MYCLOBUTANIL
METHOD: 2033 , TESTIDCODE: 61599GCM39

Laboratory ID = 20132490342 Lab Value = 0.174 Expected Conc. = 0.214 Report level label = 0.01 Pct Recovery = 81% Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20130250061 Lab Value = 0.100 Expected Conc. = 0.15 Report level label = 0.01 Pct Recovery = 67% Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl SpecificMix = A088380 Laboratory ID = 20140370077 Lab Value = 0.064 Expected Conc. = 0.107 Report level label = 0.01 Pct Recovery = 60% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20132560001 Lab Value = 0.077 Expected Conc. = 0.107 Report level label = 0.01 Pct Recovery = 72% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20132140002 Lab Value = 0.074 Expected Conc. = 0.1052 Report level label = 0.01 Pct Recovery = 71% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl SpecificMix = LB99392 Laboratory ID = 20131370001 Lab Value = 0.114 Expected Conc. = 0.1052 Report level label = 0.01 Pct Recovery = 108% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl SpecificMix = LB99392 Laboratory ID = 20140230082 Lab Value = 0.053 Expected Conc. = 0.075 Report level label = 0.01 Pct Recovery = 70% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl SpecificMix = A093651 Laboratory ID = 20132420001 Lab Value = 0.054 Expected Conc. = 0.075 Report level label = 0.01 Pct Recovery = 72% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl SpecificMix = A093651 Laboratory ID = 20130810108 Lab Value = 0.059 Expected Conc. = 0.075 Report level label = 0.01 Pct Recovery = 78% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl SpecificMix = T1120530013 Laboratory ID = 20123560092 Lab Value = 0.060 Expected Conc. = 0.075 Report level label = 0.01 Pct Recovery = 80% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = T1120530013 Laboratory ID = 20172510330 Lab Value = 0.054 Expected Conc. = 0.067 Report level label = 0.01 Pct Recovery = 81% Analysis Date = 12/29/17 SpikeMix = ChemService 6537100: 100 µl & Abs 071817Pest: 100 µl SpecificMix = 071817Pest Laboratory ID = 20162860079 Lab Value = 0.064 Expected Conc. = 0.064 Report level label = 0.01 Pct Recovery = 100% Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl SpecificMix = 060916 Laboratory ID = 20163150006 Lab Value = 0.051 Expected Conc. = 0.064 Report level label = 0.01 Pct Recovery = 80% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl SpecificMix = 060916 Laboratory ID = 20152750006 Lab Value = 0.040 Expected Conc. = 0.06 Report level label = 0.01 Pct Recovery = 67% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl SpecificMix = 040615 Laboratory ID = 20152610011 Lab Value = 0.044 Expected Conc. = 0.06 Report level label = 0.01 Pct Recovery = 73% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl SpecificMix = 040615 Laboratory ID = 20171660002 Lab Value = 0.044 Expected Conc. = 0.0512 Report level label = 0.01 Pct Recovery = 86% Analysis Date = 08/23/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = 060916 Laboratory ID = 20170190026 Lab Value = 0.049 Expected Conc. = 0.0512 Report level label = 0.01 Pct Recovery = 95% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = 060916 Laboratory ID = 20171380001 Lab Value = 0.036 Expected Conc. = 0.0504 Report level label = 0.01 Pct Recovery = 72% Analysis Date = 06/07/17 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 041816 Laboratory ID = 20170740063 Lab Value = 0.044 Expected Conc. = 0.0504 Report level label = 0.01 Pct Recovery = 87% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl SpecificMix = 041816 Laboratory ID = 20161740258 Lab Value = 0.034 Expected Conc. = 0.0504 Report level label = 0.01 Pct Recovery = 67% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 041816 Laboratory ID = 20133580036 Lab Value = 0.025 Expected Conc. = 0.0428 Report level label = 0.01 Pct Recovery = 58% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20131790009 Lab Value = 0.030 Expected Conc. = 0.0428 Report level label = 0.01 Pct Recovery = 69% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20131510026 Lab Value = 0.034 Expected Conc. = 0.0428 Report level label = 0.01 Pct Recovery = 79% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20140510043 Lab Value = 0.037 Expected Conc. = 0.0421 Report level label = 0.01 Pct Recovery = 88% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl SpecificMix = LB99392 Laboratory ID = 20133470008 Lab Value = 0.028 Expected Conc. = 0.0421 Report level label = 0.01 Pct Recovery = 67% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl SpecificMix = LB99392 Laboratory ID = 20133190012 Lab Value = 0.037 Expected Conc. = 0.0421 Report level label = 0.01 Pct Recovery = 88% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = LB99392 Laboratory ID = 20133050050 Lab Value = 0.036 Expected Conc. = 0.0421 Report level label = 0.01 Pct Recovery = 85% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl SpecificMix = LB99392 Laboratory ID = 20142720002 Lab Value = 0.032 Expected Conc. = 0.0403 Report level label = 0.01 Pct Recovery = 78% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl SpecificMix = LC06435 Laboratory ID = 20142530087 Lab Value = 0.029 Expected Conc. = 0.0403 Report level label = 0.01 Pct Recovery = 71% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl SpecificMix = LC06435 Laboratory ID = 20141570088 Lab Value = 0.031 Expected Conc. = 0.0403 Report level label = 0.01 Pct Recovery = 77% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl SpecificMix = LC06435 Laboratory ID = 20141220025 Lab Value = 0.030 Expected Conc. = 0.0403 Report level label = 0.01 Pct Recovery = 74% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl SpecificMix = LC06435 Laboratory ID = 20150720069 Lab Value = 0.042 Expected Conc. = 0.0402 Report level label = 0.01 Pct Recovery = 105% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 03DD006 Laboratory ID = 20143110108 Lab Value = 0.028 Expected Conc. = 0.0402 Report level label = 0.01 Pct Recovery = 70% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 03DD006 Laboratory ID = 20142960086 Lab Value = 0.033 Expected Conc. = 0.0402 Report level label = 0.01 Pct Recovery = 82% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 03DD006 Laboratory ID = 20142270001 Lab Value = 0.031 Expected Conc. = 0.0402 Report level label = 0.01 Pct Recovery = 76% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl SpecificMix = 03DD006 Laboratory ID = 20172560101 Lab Value = 0.031 Expected Conc. = 0.035 Report level label = 0.01 Pct Recovery = 87% Analysis Date = 12/22/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6567600: 50 µl SpecificMix = 6567600 Laboratory ID = 20161260151 Lab Value = 0.023 Expected Conc. = 0.03 Report level label = 0.01 Pct Recovery = 77% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = EN150513008 Laboratory ID = 20160770090 Lab Value = 0.021 Expected Conc. = 0.03 Report level label = 0.01 Pct Recovery = 70% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = EN150513008 Laboratory ID = 20153510109 Lab Value = 0.025 Expected Conc. = 0.03 Report level label = 0.01 Pct Recovery = 85% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = EN150513008 Laboratory ID = 20152330039 Lab Value = 0.023 Expected Conc. = 0.03 Report level label = 0.01 Pct Recovery = 75% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl SpecificMix = EN150513008 Laboratory ID = 20151900132 Lab Value = 0.034 Expected Conc. = 0.03 Report level label = 0.01 Pct Recovery = 112% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl SpecificMix = 040615 Laboratory ID = 20151550293 Lab Value = 0.030 Expected Conc. = 0.03 Report level label = 0.01 Pct Recovery = 101% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl SpecificMix = 040615 Laboratory ID = 20140860102 Lab Value = 0.020 Expected Conc. = 0.03 Report level label = 0.01 Pct Recovery = 66% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl SpecificMix = A093651 Laboratory ID = 20133400002 Lab Value = 0.022 Expected Conc. = 0.03 Report level label = 0.01 Pct Recovery = 72% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = A093651 Laboratory ID = 20132910008 Lab Value = 0.027 Expected Conc. = 0.03 Report level label = 0.01 Pct Recovery = 88% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = A093651 Laboratory ID = 20131920149 Lab Value = 0.024 Expected Conc. = 0.03 Report level label = 0.01 Pct Recovery = 81% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl SpecificMix = A093651 Laboratory ID = 20131230084 Lab Value = 0.028 Expected Conc. = 0.03 Report level label = 0.01 Pct Recovery = 92% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl SpecificMix = A088380 Laboratory ID = 20130650005 Lab Value = 0.016 Expected Conc. = 0.03 Report level label = 0.01 Pct Recovery = 53% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl SpecificMix = A088380 Laboratory ID = 20130390105 Lab Value = 0.018 Expected Conc. = 0.03 Report level label = 0.01 Pct Recovery = 61% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl SpecificMix = T1120530013 Laboratory ID = 20171160110 Lab Value = 0.024 Expected Conc. = 0.0256 Report level label = 0.01 Pct Recovery = 92% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = 060916 Laboratory ID = 20162520001 Lab Value = 0.022 Expected Conc. = 0.0256 Report level label = 0.01 Pct Recovery = 88% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl SpecificMix = 060916 Laboratory ID = 20163560019 Lab Value = 0.030 Expected Conc. = 0.0256 Report level label = 0.01 Pct Recovery = 117% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl SpecificMix = 060916 Laboratory ID = 20162380004 Lab Value = 0.020 Expected Conc. = 0.0256 Report level label = 0.01 Pct Recovery = 76% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = 060916 Laboratory ID = 20162020124 Lab Value = 0.018 Expected Conc. = 0.0252 Report level label = 0.01 Pct Recovery = 71% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl SpecificMix = 041816 Laboratory ID = 20161600087 Lab Value = 0.021 Expected Conc. = 0.0252 Report level label = 0.01 Pct Recovery = 84% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 041816 Laboratory ID = 20161340228 Lab Value = 0.019 Expected Conc. = 0.0252 Report level label = 0.01 Pct Recovery = 75% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl SpecificMix = 041816 Laboratory ID = 20161190075 Lab Value = 0.020 Expected Conc. = 0.0252 Report level label = 0.01 Pct Recovery = 79% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 041816 Laboratory ID = 20150150115 Lab Value = 0.030 Expected Conc. = 0.0202 Report level label = 0.01 Pct Recovery = 147% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl SpecificMix = LC06435 Laboratory ID = 20143370094 Lab Value = 0.018 Expected Conc. = 0.0202 Report level label = 0.01 Pct Recovery = 87% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl SpecificMix = LC06435 Laboratory ID = 20141910243 Lab Value = 0.013 Expected Conc. = 0.0202 Report level label = 0.01 Pct Recovery = 66% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = LC06435 Laboratory ID = 20141840097 Lab Value = 0.014 Expected Conc. = 0.0202 Report level label = 0.01 Pct Recovery = 70% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl SpecificMix = LC06435 Laboratory ID = 20172780018 Lab Value = 0.025 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 123% Analysis Date = 02/08/18 SpikeMix = ChemService 6537100: 30 µl & Abs 071817Pest: 30 µl SpecificMix = 071817Pest Laboratory ID = 20142200164 Lab Value = 0.016 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 82% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 03DD006 Laboratory ID = 20141640076 Lab Value = 0.012 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 60% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = 03DD006 Laboratory ID = 20141420140 Lab Value = 0.023 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 115% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 03DD006 Laboratory ID = 20141080004 Lab Value = 0.014 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 71% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl SpecificMix = 03DD006 Laboratory ID = 20161050143 Lab Value = 0.014 Expected Conc. = 0.015 Report level label = 0.01 Pct Recovery = 91% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Laboratory ID = 20160430111 Lab Value = 0.013 Expected Conc. = 0.015 Report level label = 0.01 Pct Recovery = 85% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Laboratory ID = 20160560044 Lab Value = 0.012 Expected Conc. = 0.015 Report level label = 0.01 Pct Recovery = 80% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl SpecificMix = EN150513008 Laboratory ID = 20160070059 Lab Value = 0.015 Expected Conc. = 0.015 Report level label = 0.01 Pct Recovery = 99% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = 040615 Laboratory ID = 20153160001 Lab Value = 0.014 Expected Conc. = 0.015 Report level label = 0.01 Pct Recovery = 94% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = EN150513008 Laboratory ID = 20153030068 Lab Value = 0.013 Expected Conc. = 0.015 Report level label = 0.01 Pct Recovery = 83% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150513008 Laboratory ID = 20152190003 Lab Value = 0.012 Expected Conc. = 0.015 Report level label = 0.01 Pct Recovery = 81% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150513008 Laboratory ID = 20151480170 Lab Value = 0.018 Expected Conc. = 0.015 Report level label = 0.01 Pct Recovery = 121% Analysis Date = 06/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150513008 Laboratory ID = 20151380009 Lab Value = 0.013 Expected Conc. = 0.015 Report level label = 0.01 Pct Recovery = 88% Analysis Date = 05/30/15 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Laboratory ID = 20151210037 Lab Value = 0.015 Expected Conc. = 0.015 Report level label = 0.01 Pct Recovery = 97% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Analysis Date = 02/08/18 Pct Recovery = 92% Analysis Date = 01/29/18 Pct Recovery = 92% Analysis Date = 01/29/18 Pct Recovery = 92% Analysis Date = 01/20/18 Pct Recovery = 92% Analysis Date = 01/20/18 Pct Recovery = 92% Analysis Date = 01/11/18 Pct Recovery = 92% Analysis Date = 01/11/18 Pct Recovery = 92% Analysis Date = 01/02/18 Pct Recovery = 92% Analysis Date = 01/02/18 Pct Recovery = 92% Analysis Date = 12/23/17 Pct Recovery = 91% Analysis Date = 12/23/17 Pct Recovery = 91% Analysis Date = 12/14/17 Pct Recovery = 91% Analysis Date = 12/14/17 Pct Recovery = 91% Analysis Date = 12/05/17 Pct Recovery = 91% Analysis Date = 12/05/17 Pct Recovery = 91% Analysis Date = 11/26/17 Pct Recovery = 91% Analysis Date = 11/26/17 Pct Recovery = 91% Analysis Date = 11/16/17 Pct Recovery = 91% Analysis Date = 11/16/17 Pct Recovery = 91% Analysis Date = 11/07/17 Pct Recovery = 91% Analysis Date = 11/07/17 Pct Recovery = 91% Analysis Date = 10/29/17 Pct Recovery = 91% Analysis Date = 10/29/17 Pct Recovery = 91% Analysis Date = 10/20/17 Pct Recovery = 91% Analysis Date = 10/20/17 Pct Recovery = 91% Analysis Date = 10/10/17 Pct Recovery = 90% Analysis Date = 10/10/17 Pct Recovery = 90% Analysis Date = 10/01/17 Pct Recovery = 90% Analysis Date = 10/01/17 Pct Recovery = 90% Analysis Date = 09/22/17 Pct Recovery = 90% Analysis Date = 09/22/17 Pct Recovery = 90% Analysis Date = 09/13/17 Pct Recovery = 90% Analysis Date = 09/13/17 Pct Recovery = 90% Analysis Date = 09/03/17 Pct Recovery = 90% Analysis Date = 09/03/17 Pct Recovery = 90% Analysis Date = 08/25/17 Pct Recovery = 90% Analysis Date = 08/25/17 Pct Recovery = 90% Analysis Date = 08/16/17 Pct Recovery = 90% Analysis Date = 08/16/17 Pct Recovery = 90% Analysis Date = 08/07/17 Pct Recovery = 90% Analysis Date = 08/07/17 Pct Recovery = 90% Analysis Date = 07/28/17 Pct Recovery = 89% Analysis Date = 07/28/17 Pct Recovery = 89% Analysis Date = 07/19/17 Pct Recovery = 89% Analysis Date = 07/19/17 Pct Recovery = 89% Analysis Date = 07/10/17 Pct Recovery = 89% Analysis Date = 07/10/17 Pct Recovery = 89% Analysis Date = 07/01/17 Pct Recovery = 89% Analysis Date = 07/01/17 Pct Recovery = 89% Analysis Date = 06/21/17 Pct Recovery = 89% Analysis Date = 06/21/17 Pct Recovery = 89% Analysis Date = 06/12/17 Pct Recovery = 89% Analysis Date = 06/12/17 Pct Recovery = 89% Analysis Date = 06/03/17 Pct Recovery = 89% Analysis Date = 06/03/17 Pct Recovery = 89% Analysis Date = 05/25/17 Pct Recovery = 89% Analysis Date = 05/25/17 Pct Recovery = 89% Analysis Date = 05/15/17 Pct Recovery = 88% Analysis Date = 05/15/17 Pct Recovery = 88% Analysis Date = 05/06/17 Pct Recovery = 88% Analysis Date = 05/06/17 Pct Recovery = 88% Analysis Date = 04/27/17 Pct Recovery = 88% Analysis Date = 04/27/17 Pct Recovery = 88% Analysis Date = 04/18/17 Pct Recovery = 88% Analysis Date = 04/18/17 Pct Recovery = 88% Analysis Date = 04/08/17 Pct Recovery = 88% Analysis Date = 04/08/17 Pct Recovery = 88% Analysis Date = 03/30/17 Pct Recovery = 88% Analysis Date = 03/30/17 Pct Recovery = 88% Analysis Date = 03/21/17 Pct Recovery = 88% Analysis Date = 03/21/17 Pct Recovery = 88% Analysis Date = 03/12/17 Pct Recovery = 88% Analysis Date = 03/12/17 Pct Recovery = 88% Analysis Date = 03/02/17 Pct Recovery = 87% Analysis Date = 03/02/17 Pct Recovery = 87% Analysis Date = 02/21/17 Pct Recovery = 87% Analysis Date = 02/21/17 Pct Recovery = 87% Analysis Date = 02/12/17 Pct Recovery = 87% Analysis Date = 02/12/17 Pct Recovery = 87% Analysis Date = 02/03/17 Pct Recovery = 87% Analysis Date = 02/03/17 Pct Recovery = 87% Analysis Date = 01/24/17 Pct Recovery = 87% Analysis Date = 01/24/17 Pct Recovery = 87% Analysis Date = 01/15/17 Pct Recovery = 87% Analysis Date = 01/15/17 Pct Recovery = 87% Analysis Date = 01/06/17 Pct Recovery = 87% Analysis Date = 01/06/17 Pct Recovery = 87% Analysis Date = 12/28/16 Pct Recovery = 87% Analysis Date = 12/28/16 Pct Recovery = 87% Analysis Date = 12/18/16 Pct Recovery = 87% Analysis Date = 12/18/16 Pct Recovery = 87% Analysis Date = 12/09/16 Pct Recovery = 87% Analysis Date = 12/09/16 Pct Recovery = 87% Analysis Date = 11/30/16 Pct Recovery = 87% Analysis Date = 11/30/16 Pct Recovery = 87% Analysis Date = 11/21/16 Pct Recovery = 86% Analysis Date = 11/21/16 Pct Recovery = 86% Analysis Date = 11/11/16 Pct Recovery = 86% Analysis Date = 11/11/16 Pct Recovery = 86% Analysis Date = 11/02/16 Pct Recovery = 86% Analysis Date = 11/02/16 Pct Recovery = 86% Analysis Date = 10/24/16 Pct Recovery = 86% Analysis Date = 10/24/16 Pct Recovery = 86% Analysis Date = 10/15/16 Pct Recovery = 86% Analysis Date = 10/15/16 Pct Recovery = 86% Analysis Date = 10/05/16 Pct Recovery = 86% Analysis Date = 10/05/16 Pct Recovery = 86% Analysis Date = 09/26/16 Pct Recovery = 86% Analysis Date = 09/26/16 Pct Recovery = 86% Analysis Date = 09/17/16 Pct Recovery = 86% Analysis Date = 09/17/16 Pct Recovery = 86% Analysis Date = 09/08/16 Pct Recovery = 86% Analysis Date = 09/08/16 Pct Recovery = 86% Analysis Date = 08/29/16 Pct Recovery = 86% Analysis Date = 08/29/16 Pct Recovery = 86% Analysis Date = 08/20/16 Pct Recovery = 86% Analysis Date = 08/20/16 Pct Recovery = 86% Analysis Date = 08/11/16 Pct Recovery = 86% Analysis Date = 08/11/16 Pct Recovery = 86% Analysis Date = 08/02/16 Pct Recovery = 86% Analysis Date = 08/02/16 Pct Recovery = 86% Analysis Date = 07/23/16 Pct Recovery = 86% Analysis Date = 07/23/16 Pct Recovery = 86% Analysis Date = 07/14/16 Pct Recovery = 86% Analysis Date = 07/14/16 Pct Recovery = 86% Analysis Date = 07/05/16 Pct Recovery = 86% Analysis Date = 07/05/16 Pct Recovery = 86% Analysis Date = 06/26/16 Pct Recovery = 86% Analysis Date = 06/26/16 Pct Recovery = 86% Analysis Date = 06/16/16 Pct Recovery = 86% Analysis Date = 06/16/16 Pct Recovery = 86% Analysis Date = 06/07/16 Pct Recovery = 86% Analysis Date = 06/07/16 Pct Recovery = 86% Analysis Date = 05/29/16 Pct Recovery = 86% Analysis Date = 05/29/16 Pct Recovery = 86% Analysis Date = 05/20/16 Pct Recovery = 86% Analysis Date = 05/20/16 Pct Recovery = 86% Analysis Date = 05/10/16 Pct Recovery = 86% Analysis Date = 05/10/16 Pct Recovery = 86% Analysis Date = 05/01/16 Pct Recovery = 86% Analysis Date = 05/01/16 Pct Recovery = 86% Analysis Date = 04/22/16 Pct Recovery = 86% Analysis Date = 04/22/16 Pct Recovery = 86% Analysis Date = 04/13/16 Pct Recovery = 86% Analysis Date = 04/13/16 Pct Recovery = 86% Analysis Date = 04/03/16 Pct Recovery = 86% Analysis Date = 04/03/16 Pct Recovery = 86% Analysis Date = 03/25/16 Pct Recovery = 86% Analysis Date = 03/25/16 Pct Recovery = 86% Analysis Date = 03/16/16 Pct Recovery = 86% Analysis Date = 03/16/16 Pct Recovery = 86% Analysis Date = 03/07/16 Pct Recovery = 87% Analysis Date = 03/07/16 Pct Recovery = 87% Analysis Date = 02/26/16 Pct Recovery = 87% Analysis Date = 02/26/16 Pct Recovery = 87% Analysis Date = 02/17/16 Pct Recovery = 87% Analysis Date = 02/17/16 Pct Recovery = 87% Analysis Date = 02/08/16 Pct Recovery = 87% Analysis Date = 02/08/16 Pct Recovery = 87% Analysis Date = 01/30/16 Pct Recovery = 87% Analysis Date = 01/30/16 Pct Recovery = 87% Analysis Date = 01/20/16 Pct Recovery = 87% Analysis Date = 01/20/16 Pct Recovery = 87% Analysis Date = 01/11/16 Pct Recovery = 87% Analysis Date = 01/11/16 Pct Recovery = 87% Analysis Date = 01/02/16 Pct Recovery = 87% Analysis Date = 01/02/16 Pct Recovery = 87% Analysis Date = 12/24/15 Pct Recovery = 87% Analysis Date = 12/24/15 Pct Recovery = 87% Analysis Date = 12/14/15 Pct Recovery = 88% Analysis Date = 12/14/15 Pct Recovery = 88% Analysis Date = 12/05/15 Pct Recovery = 88% Analysis Date = 12/05/15 Pct Recovery = 88% Analysis Date = 11/26/15 Pct Recovery = 88% Analysis Date = 11/26/15 Pct Recovery = 88% Analysis Date = 11/17/15 Pct Recovery = 88% Analysis Date = 11/17/15 Pct Recovery = 88% Analysis Date = 11/07/15 Pct Recovery = 88% Analysis Date = 11/07/15 Pct Recovery = 88% Analysis Date = 10/29/15 Pct Recovery = 88% Analysis Date = 10/29/15 Pct Recovery = 88% Analysis Date = 10/20/15 Pct Recovery = 88% Analysis Date = 10/20/15 Pct Recovery = 88% Analysis Date = 10/11/15 Pct Recovery = 88% Analysis Date = 10/11/15 Pct Recovery = 88% Analysis Date = 10/01/15 Pct Recovery = 88% Analysis Date = 10/01/15 Pct Recovery = 88% Analysis Date = 09/22/15 Pct Recovery = 88% Analysis Date = 09/22/15 Pct Recovery = 88% Analysis Date = 09/13/15 Pct Recovery = 88% Analysis Date = 09/13/15 Pct Recovery = 88% Analysis Date = 09/04/15 Pct Recovery = 88% Analysis Date = 09/04/15 Pct Recovery = 88% Analysis Date = 08/25/15 Pct Recovery = 88% Analysis Date = 08/25/15 Pct Recovery = 88% Analysis Date = 08/16/15 Pct Recovery = 88% Analysis Date = 08/16/15 Pct Recovery = 88% Analysis Date = 08/07/15 Pct Recovery = 88% Analysis Date = 08/07/15 Pct Recovery = 88% Analysis Date = 07/29/15 Pct Recovery = 88% Analysis Date = 07/29/15 Pct Recovery = 88% Analysis Date = 07/19/15 Pct Recovery = 88% Analysis Date = 07/19/15 Pct Recovery = 88% Analysis Date = 07/10/15 Pct Recovery = 88% Analysis Date = 07/10/15 Pct Recovery = 88% Analysis Date = 07/01/15 Pct Recovery = 88% Analysis Date = 07/01/15 Pct Recovery = 88% Analysis Date = 06/22/15 Pct Recovery = 88% Analysis Date = 06/22/15 Pct Recovery = 88% Analysis Date = 06/12/15 Pct Recovery = 88% Analysis Date = 06/12/15 Pct Recovery = 88% Analysis Date = 06/03/15 Pct Recovery = 88% Analysis Date = 06/03/15 Pct Recovery = 88% Analysis Date = 05/25/15 Pct Recovery = 88% Analysis Date = 05/25/15 Pct Recovery = 88% Analysis Date = 05/16/15 Pct Recovery = 88% Analysis Date = 05/16/15 Pct Recovery = 88% Analysis Date = 05/06/15 Pct Recovery = 88% Analysis Date = 05/06/15 Pct Recovery = 88% Analysis Date = 04/27/15 Pct Recovery = 88% Analysis Date = 04/27/15 Pct Recovery = 88% Analysis Date = 04/18/15 Pct Recovery = 88% Analysis Date = 04/18/15 Pct Recovery = 88% Analysis Date = 04/09/15 Pct Recovery = 88% Analysis Date = 04/09/15 Pct Recovery = 88% Analysis Date = 03/30/15 Pct Recovery = 88% Analysis Date = 03/30/15 Pct Recovery = 88% Analysis Date = 03/21/15 Pct Recovery = 88% Analysis Date = 03/21/15 Pct Recovery = 88% Analysis Date = 03/12/15 Pct Recovery = 88% Analysis Date = 03/12/15 Pct Recovery = 88% Analysis Date = 03/03/15 Pct Recovery = 88% Analysis Date = 03/03/15 Pct Recovery = 88% Analysis Date = 02/21/15 Pct Recovery = 88% Analysis Date = 02/21/15 Pct Recovery = 88% Analysis Date = 02/12/15 Pct Recovery = 87% Analysis Date = 02/12/15 Pct Recovery = 87% Analysis Date = 02/03/15 Pct Recovery = 87% Analysis Date = 02/03/15 Pct Recovery = 87% Analysis Date = 01/25/15 Pct Recovery = 87% Analysis Date = 01/25/15 Pct Recovery = 87% Analysis Date = 01/15/15 Pct Recovery = 87% Analysis Date = 01/15/15 Pct Recovery = 87% Analysis Date = 01/06/15 Pct Recovery = 87% Analysis Date = 01/06/15 Pct Recovery = 87% Analysis Date = 12/28/14 Pct Recovery = 87% Analysis Date = 12/28/14 Pct Recovery = 87% Analysis Date = 12/19/14 Pct Recovery = 87% Analysis Date = 12/19/14 Pct Recovery = 87% Analysis Date = 12/09/14 Pct Recovery = 87% Analysis Date = 12/09/14 Pct Recovery = 87% Analysis Date = 11/30/14 Pct Recovery = 87% Analysis Date = 11/30/14 Pct Recovery = 87% Analysis Date = 11/21/14 Pct Recovery = 86% Analysis Date = 11/21/14 Pct Recovery = 86% Analysis Date = 11/12/14 Pct Recovery = 86% Analysis Date = 11/12/14 Pct Recovery = 86% Analysis Date = 11/02/14 Pct Recovery = 85% Analysis Date = 11/02/14 Pct Recovery = 85% Analysis Date = 10/24/14 Pct Recovery = 85% Analysis Date = 10/24/14 Pct Recovery = 85% Analysis Date = 10/15/14 Pct Recovery = 85% Analysis Date = 10/15/14 Pct Recovery = 85% Analysis Date = 10/06/14 Pct Recovery = 84% Analysis Date = 10/06/14 Pct Recovery = 84% Analysis Date = 09/26/14 Pct Recovery = 84% Analysis Date = 09/26/14 Pct Recovery = 84% Analysis Date = 09/17/14 Pct Recovery = 84% Analysis Date = 09/17/14 Pct Recovery = 84% Analysis Date = 09/08/14 Pct Recovery = 83% Analysis Date = 09/08/14 Pct Recovery = 83% Analysis Date = 08/30/14 Pct Recovery = 83% Analysis Date = 08/30/14 Pct Recovery = 83% Analysis Date = 08/20/14 Pct Recovery = 83% Analysis Date = 08/20/14 Pct Recovery = 83% Analysis Date = 08/11/14 Pct Recovery = 82% Analysis Date = 08/11/14 Pct Recovery = 82% Analysis Date = 08/02/14 Pct Recovery = 82% Analysis Date = 08/02/14 Pct Recovery = 82% Analysis Date = 07/24/14 Pct Recovery = 81% Analysis Date = 07/24/14 Pct Recovery = 81% Analysis Date = 07/14/14 Pct Recovery = 81% Analysis Date = 07/14/14 Pct Recovery = 81% Analysis Date = 07/05/14 Pct Recovery = 81% Analysis Date = 07/05/14 Pct Recovery = 81% Analysis Date = 06/26/14 Pct Recovery = 80% Analysis Date = 06/26/14 Pct Recovery = 80% Analysis Date = 06/17/14 Pct Recovery = 80% Analysis Date = 06/17/14 Pct Recovery = 80% Analysis Date = 06/07/14 Pct Recovery = 80% Analysis Date = 06/07/14 Pct Recovery = 80% Analysis Date = 05/29/14 Pct Recovery = 79% Analysis Date = 05/29/14 Pct Recovery = 79% Analysis Date = 05/20/14 Pct Recovery = 79% Analysis Date = 05/20/14 Pct Recovery = 79% Analysis Date = 05/11/14 Pct Recovery = 79% Analysis Date = 05/11/14 Pct Recovery = 79% Analysis Date = 05/01/14 Pct Recovery = 78% Analysis Date = 05/01/14 Pct Recovery = 78% Analysis Date = 04/22/14 Pct Recovery = 78% Analysis Date = 04/22/14 Pct Recovery = 78% Analysis Date = 04/13/14 Pct Recovery = 78% Analysis Date = 04/13/14 Pct Recovery = 78% Analysis Date = 04/04/14 Pct Recovery = 78% Analysis Date = 04/04/14 Pct Recovery = 78% Analysis Date = 03/25/14 Pct Recovery = 77% Analysis Date = 03/25/14 Pct Recovery = 77% Analysis Date = 03/16/14 Pct Recovery = 77% Analysis Date = 03/16/14 Pct Recovery = 77% Analysis Date = 03/07/14 Pct Recovery = 77% Analysis Date = 03/07/14 Pct Recovery = 77% Analysis Date = 02/26/14 Pct Recovery = 77% Analysis Date = 02/26/14 Pct Recovery = 77% Analysis Date = 02/16/14 Pct Recovery = 77% Analysis Date = 02/16/14 Pct Recovery = 77% Analysis Date = 02/07/14 Pct Recovery = 77% Analysis Date = 02/07/14 Pct Recovery = 77% Analysis Date = 01/29/14 Pct Recovery = 77% Analysis Date = 01/29/14 Pct Recovery = 77% Analysis Date = 01/20/14 Pct Recovery = 77% Analysis Date = 01/20/14 Pct Recovery = 77% Analysis Date = 01/10/14 Pct Recovery = 77% Analysis Date = 01/10/14 Pct Recovery = 77% Analysis Date = 01/01/14 Pct Recovery = 77% Analysis Date = 01/01/14 Pct Recovery = 77% Analysis Date = 12/23/13 Pct Recovery = 77% Analysis Date = 12/23/13 Pct Recovery = 77% Analysis Date = 12/14/13 Pct Recovery = 77% Analysis Date = 12/14/13 Pct Recovery = 77% Analysis Date = 12/04/13 Pct Recovery = 77% Analysis Date = 12/04/13 Pct Recovery = 77% Analysis Date = 11/25/13 Pct Recovery = 76% Analysis Date = 11/25/13 Pct Recovery = 76% Analysis Date = 11/16/13 Pct Recovery = 76% Analysis Date = 11/16/13 Pct Recovery = 76% Analysis Date = 11/07/13 Pct Recovery = 76% Analysis Date = 11/07/13 Pct Recovery = 76% Analysis Date = 10/28/13 Pct Recovery = 76% Analysis Date = 10/28/13 Pct Recovery = 76% Analysis Date = 10/19/13 Pct Recovery = 76% Analysis Date = 10/19/13 Pct Recovery = 76% Analysis Date = 10/10/13 Pct Recovery = 76% Analysis Date = 10/10/13 Pct Recovery = 76% Analysis Date = 10/01/13 Pct Recovery = 76% Analysis Date = 10/01/13 Pct Recovery = 76% Analysis Date = 09/21/13 Pct Recovery = 76% Analysis Date = 09/21/13 Pct Recovery = 76% Analysis Date = 09/12/13 Pct Recovery = 76% Analysis Date = 09/12/13 Pct Recovery = 76% Analysis Date = 09/03/13 Pct Recovery = 76% Analysis Date = 09/03/13 Pct Recovery = 76% Analysis Date = 08/25/13 Pct Recovery = 76% Analysis Date = 08/25/13 Pct Recovery = 76% Analysis Date = 08/15/13 Pct Recovery = 76% Analysis Date = 08/15/13 Pct Recovery = 76% Analysis Date = 08/06/13 Pct Recovery = 76% Analysis Date = 08/06/13 Pct Recovery = 76% Analysis Date = 07/28/13 Pct Recovery = 75% Analysis Date = 07/28/13 Pct Recovery = 75% Analysis Date = 07/19/13 Pct Recovery = 75% Analysis Date = 07/19/13 Pct Recovery = 75% Analysis Date = 07/09/13 Pct Recovery = 75% Analysis Date = 07/09/13 Pct Recovery = 75% Analysis Date = 06/30/13 Pct Recovery = 75% Analysis Date = 06/30/13 Pct Recovery = 75% Analysis Date = 06/21/13 Pct Recovery = 75% Analysis Date = 06/21/13 Pct Recovery = 75% Analysis Date = 06/12/13 Pct Recovery = 75% Analysis Date = 06/12/13 Pct Recovery = 75% Analysis Date = 06/02/13 Pct Recovery = 75% Analysis Date = 06/02/13 Pct Recovery = 75% Analysis Date = 05/24/13 Pct Recovery = 75% Analysis Date = 05/24/13 Pct Recovery = 75% Analysis Date = 05/15/13 Pct Recovery = 75% Analysis Date = 05/15/13 Pct Recovery = 75% Analysis Date = 05/06/13 Pct Recovery = 75% Analysis Date = 05/06/13 Pct Recovery = 75% Analysis Date = 04/26/13 Pct Recovery = 75% Analysis Date = 04/26/13 Pct Recovery = 75% Analysis Date = 04/17/13 Pct Recovery = 75% Analysis Date = 04/17/13 Pct Recovery = 75% Analysis Date = 04/08/13 Pct Recovery = 75% Analysis Date = 04/08/13 Pct Recovery = 75% Analysis Date = 03/30/13 Pct Recovery = 75% Analysis Date = 03/30/13 Pct Recovery = 75% Analysis Date = 03/20/13 Pct Recovery = 75% Analysis Date = 03/20/13 Pct Recovery = 75% Analysis Date = 03/11/13 Pct Recovery = 75% Analysis Date = 03/11/13 Pct Recovery = 75% Analysis Date = 03/02/13 Pct Recovery = 75% Analysis Date = 03/02/13 Pct Recovery = 75% Analysis Date = 02/21/13 Pct Recovery = 75% Analysis Date = 02/21/13 Pct Recovery = 75% Analysis Date = 02/11/13 Pct Recovery = 75% Analysis Date = 02/11/13 Pct Recovery = 75% Analysis Date = 02/02/13 Pct Recovery = 75% Analysis Date = 02/02/13 Pct Recovery = 75% Analysis Date = 01/24/13 Pct Recovery = 75% Analysis Date = 01/24/13 Pct Recovery = 75% Analysis Date = 01/15/13 Pct Recovery = 75% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
MYCLOBUTANIL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 76 83% 16% 80% 13%
Total 76 83% 16% 80% 13%

Sample Statistics
MYCLOBUTANIL

Characteristic N % % Basis
Plotted 76 100% Spiked
Estimated Values 1 1% Spiked
Deleted Values 2 2% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 77 .  
False Negatives 0 0% 0 out of 76
Not Spiked 41 .  
False Positives 0 0% 0 out of 40

OBSP Determination:
OXYFLUORFEN
METHOD: 2033 , TESTIDCODE: 61600GCM39

Laboratory ID = 20130250061 Lab Value = 0.139 Expected Conc. = 0.3 Report level label = 0.01 Pct Recovery = 46% Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl SpecificMix = A088380 Laboratory ID = 20140230082 Lab Value = 0.084 Expected Conc. = 0.15 Report level label = 0.01 Pct Recovery = 56% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl SpecificMix = A093651 Laboratory ID = 20132420001 Lab Value = 0.102 Expected Conc. = 0.15 Report level label = 0.01 Pct Recovery = 68% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl SpecificMix = A093651 Laboratory ID = 20130810108 Lab Value = 0.089 Expected Conc. = 0.15 Report level label = 0.01 Pct Recovery = 59% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl SpecificMix = T1120530013 Laboratory ID = 20123560092 Lab Value = 0.099 Expected Conc. = 0.15 Report level label = 0.01 Pct Recovery = 66% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = T1120530013 Laboratory ID = 20140100085 Lab Value = 0.079 Expected Conc. = 0.12 Report level label = 0.01 Pct Recovery = 66% Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl SpecificMix = T1130514013 Laboratory ID = 20132490342 Lab Value = 0.087 Expected Conc. = 0.12 Report level label = 0.01 Pct Recovery = 73% Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl SpecificMix = T1130514013 Laboratory ID = 20163370001 Lab Value = 0.061 Expected Conc. = 0.0625 Report level label = 0.01 Pct Recovery = 97% Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl SpecificMix = LC20138V Laboratory ID = 20162860079 Lab Value = 0.052 Expected Conc. = 0.06 Report level label = 0.01 Pct Recovery = 86% Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl SpecificMix = 5054800 Laboratory ID = 20161880109 Lab Value = 0.062 Expected Conc. = 0.06 Report level label = 0.01 Pct Recovery = 103% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl SpecificMix = 5054800 Laboratory ID = 20152750006 Lab Value = 0.050 Expected Conc. = 0.06 Report level label = 0.01 Pct Recovery = 84% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl SpecificMix = 040615 Laboratory ID = 20152610011 Lab Value = 0.053 Expected Conc. = 0.06 Report level label = 0.01 Pct Recovery = 89% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl SpecificMix = 040615 Laboratory ID = 20140860102 Lab Value = 0.041 Expected Conc. = 0.06 Report level label = 0.01 Pct Recovery = 68% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl SpecificMix = A093651 Laboratory ID = 20140370077 Lab Value = 0.043 Expected Conc. = 0.06 Report level label = 0.01 Pct Recovery = 71% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl SpecificMix = T1130514013 Laboratory ID = 20133400002 Lab Value = 0.044 Expected Conc. = 0.06 Report level label = 0.01 Pct Recovery = 74% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = A093651 Laboratory ID = 20132910008 Lab Value = 0.053 Expected Conc. = 0.06 Report level label = 0.01 Pct Recovery = 88% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = A093651 Laboratory ID = 20132690010 Lab Value = 0.051 Expected Conc. = 0.06 Report level label = 0.01 Pct Recovery = 85% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl SpecificMix = T1130514013 Laboratory ID = 20131920149 Lab Value = 0.051 Expected Conc. = 0.06 Report level label = 0.01 Pct Recovery = 85% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl SpecificMix = A093651 Laboratory ID = 20131370001 Lab Value = 0.053 Expected Conc. = 0.06 Report level label = 0.01 Pct Recovery = 89% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl SpecificMix = 1473000 Laboratory ID = 20131230084 Lab Value = 0.046 Expected Conc. = 0.06 Report level label = 0.01 Pct Recovery = 76% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl SpecificMix = A088380 Laboratory ID = 20130650005 Lab Value = 0.036 Expected Conc. = 0.06 Report level label = 0.01 Pct Recovery = 61% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl SpecificMix = A088380 Laboratory ID = 20130390105 Lab Value = 0.040 Expected Conc. = 0.06 Report level label = 0.01 Pct Recovery = 67% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl SpecificMix = T1120530013 Laboratory ID = 20171720140 Lab Value = 0.039 Expected Conc. = 0.05 Report level label = 0.01 Pct Recovery = 78% Analysis Date = 08/31/17 SpikeMix = Supelco LC20138V: 80 µl & Phenova B20160331: 80 µl SpecificMix = LC20138V Laboratory ID = 20170740063 Lab Value = 0.045 Expected Conc. = 0.05 Report level label = 0.01 Pct Recovery = 90% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl SpecificMix = LC20138V Laboratory ID = 20161470001 Lab Value = 0.036 Expected Conc. = 0.05 Report level label = 0.01 Pct Recovery = 73% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl SpecificMix = LC20138V Laboratory ID = 20171380001 Lab Value = 0.050 Expected Conc. = 0.048 Report level label = 0.01 Pct Recovery = 104% Analysis Date = 06/07/17 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 5054800 Laboratory ID = 20170960001 Lab Value = 0.043 Expected Conc. = 0.048 Report level label = 0.01 Pct Recovery = 89% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl SpecificMix = 5054800 Laboratory ID = 20161740258 Lab Value = 0.049 Expected Conc. = 0.048 Report level label = 0.01 Pct Recovery = 102% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 5054800 Laboratory ID = 20150720069 Lab Value = 0.038 Expected Conc. = 0.0402 Report level label = 0.01 Pct Recovery = 95% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 03DD006 Laboratory ID = 20143110108 Lab Value = 0.039 Expected Conc. = 0.0402 Report level label = 0.01 Pct Recovery = 98% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 03DD006 Laboratory ID = 20142960086 Lab Value = 0.035 Expected Conc. = 0.0402 Report level label = 0.01 Pct Recovery = 87% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 03DD006 Laboratory ID = 20142720002 Lab Value = 0.040 Expected Conc. = 0.0402 Report level label = 0.01 Pct Recovery = 98% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl SpecificMix = LC06435 Laboratory ID = 20142530087 Lab Value = 0.034 Expected Conc. = 0.0402 Report level label = 0.01 Pct Recovery = 85% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl SpecificMix = LC06435 Laboratory ID = 20142270001 Lab Value = 0.035 Expected Conc. = 0.0402 Report level label = 0.01 Pct Recovery = 88% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl SpecificMix = 03DD006 Laboratory ID = 20141570088 Lab Value = 0.026 Expected Conc. = 0.0402 Report level label = 0.01 Pct Recovery = 65% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl SpecificMix = LC06435 Laboratory ID = 20141220025 Lab Value = 0.034 Expected Conc. = 0.0402 Report level label = 0.01 Pct Recovery = 85% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl SpecificMix = LC06435 Laboratory ID = 20172230001 Lab Value = 0.028 Expected Conc. = 0.035 Report level label = 0.01 Pct Recovery = 81% Analysis Date = 10/19/17 SpikeMix = ChemService 6472100: 50 µl & Abs 071717Pest: 50 µl SpecificMix = 6472100 Laboratory ID = 20172560101 Lab Value = 0.039 Expected Conc. = 0.033 Report level label = 0.01 Pct Recovery = 117% Analysis Date = 12/22/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6567600: 50 µl SpecificMix = EN170808006 Laboratory ID = 20172370001 Lab Value = 0.044 Expected Conc. = 0.033 Report level label = 0.01 Pct Recovery = 133% Analysis Date = 11/18/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6537100: 50 µl SpecificMix = EN170808006 Laboratory ID = 20161260151 Lab Value = 0.031 Expected Conc. = 0.03 Report level label = 0.01 Pct Recovery = 103% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = EN150513008 Laboratory ID = 20160770090 Lab Value = 0.024 Expected Conc. = 0.03 Report level label = 0.01 Pct Recovery = 78% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = EN150513008 Laboratory ID = 20153510109 Lab Value = 0.021 Expected Conc. = 0.03 Report level label = 0.01 Pct Recovery = 71% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = EN150513008 Laboratory ID = 20152330039 Lab Value = 0.024 Expected Conc. = 0.03 Report level label = 0.01 Pct Recovery = 81% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl SpecificMix = EN150513008 Laboratory ID = 20151900132 Lab Value = 0.025 Expected Conc. = 0.03 Report level label = 0.01 Pct Recovery = 82% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl SpecificMix = 040615 Laboratory ID = 20151550293 Lab Value = 0.028 Expected Conc. = 0.03 Report level label = 0.01 Pct Recovery = 93% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl SpecificMix = 040615 Laboratory ID = 20171510080 Lab Value = 0.020 Expected Conc. = 0.025 Report level label = 0.01 Pct Recovery = 80% Analysis Date = 06/09/17 SpikeMix = Supelco LC20138V: 40 µl & Crescent 03FF076: 40 µl SpecificMix = LC20138V Laboratory ID = 20162520001 Lab Value = 0.022 Expected Conc. = 0.025 Report level label = 0.01 Pct Recovery = 86% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl SpecificMix = LC20138V Laboratory ID = 20162660005 Lab Value = 0.022 Expected Conc. = 0.025 Report level label = 0.01 Pct Recovery = 89% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl SpecificMix = LC20138V Laboratory ID = 20162020124 Lab Value = 0.024 Expected Conc. = 0.025 Report level label = 0.01 Pct Recovery = 94% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl SpecificMix = LC20138V Laboratory ID = 20171940002 Lab Value = 0.031 Expected Conc. = 0.024 Report level label = 0.01 Pct Recovery = 128% Analysis Date = 11/10/17 SpikeMix = ChemService 5054800: 40 µl & NSI 041816: 40 µl SpecificMix = 5054800 Laboratory ID = 20170460061 Lab Value = 0.024 Expected Conc. = 0.024 Report level label = 0.01 Pct Recovery = 101% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl SpecificMix = 5054800 Laboratory ID = 20163560019 Lab Value = 0.033 Expected Conc. = 0.024 Report level label = 0.01 Pct Recovery = 137% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl SpecificMix = 5054800 Laboratory ID = 20162150213 Lab Value = 0.043 Expected Conc. = 0.024 Report level label = 0.01 Pct Recovery = 178% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl SpecificMix = 5054800 Laboratory ID = 20140730138 Lab Value = 0.020 Expected Conc. = 0.024 Report level label = 0.01 Pct Recovery = 83% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 1473000 Laboratory ID = 20133470008 Lab Value = 0.022 Expected Conc. = 0.024 Report level label = 0.01 Pct Recovery = 92% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl SpecificMix = 1473000 Laboratory ID = 20133310030 Lab Value = 0.029 Expected Conc. = 0.024 Report level label = 0.01 Pct Recovery = 122% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl SpecificMix = 1473000 Laboratory ID = 20133050050 Lab Value = 0.020 Expected Conc. = 0.024 Report level label = 0.01 Pct Recovery = 84% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl SpecificMix = T1130514013 Laboratory ID = 20132280016 Lab Value = 0.023 Expected Conc. = 0.024 Report level label = 0.01 Pct Recovery = 96% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl SpecificMix = T1130514013 Laboratory ID = 20131790009 Lab Value = 0.026 Expected Conc. = 0.024 Report level label = 0.01 Pct Recovery = 110% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl SpecificMix = 1473000 Laboratory ID = 20131650073 Lab Value = 0.020 Expected Conc. = 0.024 Report level label = 0.01 Pct Recovery = 84% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl SpecificMix = 1473000 Laboratory ID = 20173120093 Lab Value = 0.021 Expected Conc. = 0.021 Report level label = 0.01 Pct Recovery = 99% Analysis Date = 03/10/18 SpikeMix = ChemService 6472100: 30 µl & ChemService 6537100: 30 µl SpecificMix = 6472100 Laboratory ID = 20150150115 Lab Value = 0.022 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 111% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl SpecificMix = LC06435 Laboratory ID = 20143370094 Lab Value = 0.024 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 121% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl SpecificMix = LC06435 Laboratory ID = 20142200164 Lab Value = 0.021 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 102% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 03DD006 Laboratory ID = 20141910243 Lab Value = 0.016 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 82% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = LC06435 Laboratory ID = 20141840097 Lab Value = 0.018 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 89% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl SpecificMix = LC06435 Laboratory ID = 20141640076 Lab Value = 0.014 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 72% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = 03DD006 Laboratory ID = 20141420140 Lab Value = 0.016 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 80% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 03DD006 Laboratory ID = 20141080004 Lab Value = 0.018 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 88% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl SpecificMix = 03DD006 Laboratory ID = 20161050143 Lab Value = 0.013 Expected Conc. = 0.015 Report level label = 0.01 Pct Recovery = 87% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Laboratory ID = 20160430111 Lab Value = 0.014 Expected Conc. = 0.015 Report level label = 0.01 Pct Recovery = 93% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Laboratory ID = 20160560044 Lab Value = 0.014 Expected Conc. = 0.015 Report level label = 0.01 Pct Recovery = 95% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl SpecificMix = EN150513008 Laboratory ID = 20160070059 Lab Value = 0.011 Expected Conc. = 0.015 Report level label = 0.01 Pct Recovery = 71% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = 040615 Laboratory ID = 20153160001 Lab Value = 0.016 Expected Conc. = 0.015 Report level label = 0.01 Pct Recovery = 105% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = EN150513008 Laboratory ID = 20153030068 Lab Value = 0.016 Expected Conc. = 0.015 Report level label = 0.01 Pct Recovery = 106% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150513008 Laboratory ID = 20152190003 Lab Value = 0.014 Expected Conc. = 0.015 Report level label = 0.01 Pct Recovery = 91% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150513008 Laboratory ID = 20151480170 Lab Value = 0.015 Expected Conc. = 0.015 Report level label = 0.01 Pct Recovery = 98% Analysis Date = 06/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150513008 Laboratory ID = 20151380009 Lab Value = 0.013 Expected Conc. = 0.015 Report level label = 0.01 Pct Recovery = 89% Analysis Date = 05/30/15 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Laboratory ID = 20151210037 Lab Value = 0.013 Expected Conc. = 0.015 Report level label = 0.01 Pct Recovery = 89% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Analysis Date = 03/10/18 Pct Recovery = 107% Analysis Date = 02/28/18 Pct Recovery = 106% Analysis Date = 02/28/18 Pct Recovery = 106% Analysis Date = 02/19/18 Pct Recovery = 106% Analysis Date = 02/19/18 Pct Recovery = 106% Analysis Date = 02/09/18 Pct Recovery = 106% Analysis Date = 02/09/18 Pct Recovery = 106% Analysis Date = 01/31/18 Pct Recovery = 106% Analysis Date = 01/31/18 Pct Recovery = 106% Analysis Date = 01/22/18 Pct Recovery = 106% Analysis Date = 01/22/18 Pct Recovery = 106% Analysis Date = 01/12/18 Pct Recovery = 106% Analysis Date = 01/12/18 Pct Recovery = 106% Analysis Date = 01/03/18 Pct Recovery = 105% Analysis Date = 01/03/18 Pct Recovery = 105% Analysis Date = 12/24/17 Pct Recovery = 105% Analysis Date = 12/24/17 Pct Recovery = 105% Analysis Date = 12/15/17 Pct Recovery = 105% Analysis Date = 12/15/17 Pct Recovery = 105% Analysis Date = 12/06/17 Pct Recovery = 105% Analysis Date = 12/06/17 Pct Recovery = 105% Analysis Date = 11/26/17 Pct Recovery = 105% Analysis Date = 11/26/17 Pct Recovery = 105% Analysis Date = 11/17/17 Pct Recovery = 105% Analysis Date = 11/17/17 Pct Recovery = 105% Analysis Date = 11/07/17 Pct Recovery = 104% Analysis Date = 11/07/17 Pct Recovery = 104% Analysis Date = 10/29/17 Pct Recovery = 104% Analysis Date = 10/29/17 Pct Recovery = 104% Analysis Date = 10/20/17 Pct Recovery = 104% Analysis Date = 10/20/17 Pct Recovery = 104% Analysis Date = 10/10/17 Pct Recovery = 104% Analysis Date = 10/10/17 Pct Recovery = 104% Analysis Date = 10/01/17 Pct Recovery = 104% Analysis Date = 10/01/17 Pct Recovery = 104% Analysis Date = 09/21/17 Pct Recovery = 104% Analysis Date = 09/21/17 Pct Recovery = 104% Analysis Date = 09/12/17 Pct Recovery = 103% Analysis Date = 09/12/17 Pct Recovery = 103% Analysis Date = 09/03/17 Pct Recovery = 103% Analysis Date = 09/03/17 Pct Recovery = 103% Analysis Date = 08/24/17 Pct Recovery = 103% Analysis Date = 08/24/17 Pct Recovery = 103% Analysis Date = 08/15/17 Pct Recovery = 103% Analysis Date = 08/15/17 Pct Recovery = 103% Analysis Date = 08/05/17 Pct Recovery = 103% Analysis Date = 08/05/17 Pct Recovery = 103% Analysis Date = 07/27/17 Pct Recovery = 103% Analysis Date = 07/27/17 Pct Recovery = 103% Analysis Date = 07/18/17 Pct Recovery = 102% Analysis Date = 07/18/17 Pct Recovery = 102% Analysis Date = 07/08/17 Pct Recovery = 102% Analysis Date = 07/08/17 Pct Recovery = 102% Analysis Date = 06/29/17 Pct Recovery = 102% Analysis Date = 06/29/17 Pct Recovery = 102% Analysis Date = 06/19/17 Pct Recovery = 102% Analysis Date = 06/19/17 Pct Recovery = 102% Analysis Date = 06/10/17 Pct Recovery = 102% Analysis Date = 06/10/17 Pct Recovery = 102% Analysis Date = 06/01/17 Pct Recovery = 101% Analysis Date = 06/01/17 Pct Recovery = 101% Analysis Date = 05/22/17 Pct Recovery = 101% Analysis Date = 05/22/17 Pct Recovery = 101% Analysis Date = 05/13/17 Pct Recovery = 101% Analysis Date = 05/13/17 Pct Recovery = 101% Analysis Date = 05/03/17 Pct Recovery = 101% Analysis Date = 05/03/17 Pct Recovery = 101% Analysis Date = 04/24/17 Pct Recovery = 101% Analysis Date = 04/24/17 Pct Recovery = 101% Analysis Date = 04/15/17 Pct Recovery = 101% Analysis Date = 04/15/17 Pct Recovery = 101% Analysis Date = 04/05/17 Pct Recovery = 100% Analysis Date = 04/05/17 Pct Recovery = 100% Analysis Date = 03/27/17 Pct Recovery = 100% Analysis Date = 03/27/17 Pct Recovery = 100% Analysis Date = 03/17/17 Pct Recovery = 100% Analysis Date = 03/17/17 Pct Recovery = 100% Analysis Date = 03/08/17 Pct Recovery = 100% Analysis Date = 03/08/17 Pct Recovery = 100% Analysis Date = 02/27/17 Pct Recovery = 100% Analysis Date = 02/27/17 Pct Recovery = 100% Analysis Date = 02/17/17 Pct Recovery = 100% Analysis Date = 02/17/17 Pct Recovery = 100% Analysis Date = 02/08/17 Pct Recovery = 99% Analysis Date = 02/08/17 Pct Recovery = 99% Analysis Date = 01/29/17 Pct Recovery = 99% Analysis Date = 01/29/17 Pct Recovery = 99% Analysis Date = 01/20/17 Pct Recovery = 99% Analysis Date = 01/20/17 Pct Recovery = 99% Analysis Date = 01/11/17 Pct Recovery = 99% Analysis Date = 01/11/17 Pct Recovery = 99% Analysis Date = 01/01/17 Pct Recovery = 99% Analysis Date = 01/01/17 Pct Recovery = 99% Analysis Date = 12/23/16 Pct Recovery = 98% Analysis Date = 12/23/16 Pct Recovery = 98% Analysis Date = 12/13/16 Pct Recovery = 98% Analysis Date = 12/13/16 Pct Recovery = 98% Analysis Date = 12/04/16 Pct Recovery = 98% Analysis Date = 12/04/16 Pct Recovery = 98% Analysis Date = 11/25/16 Pct Recovery = 98% Analysis Date = 11/25/16 Pct Recovery = 98% Analysis Date = 11/15/16 Pct Recovery = 98% Analysis Date = 11/15/16 Pct Recovery = 98% Analysis Date = 11/06/16 Pct Recovery = 98% Analysis Date = 11/06/16 Pct Recovery = 98% Analysis Date = 10/27/16 Pct Recovery = 97% Analysis Date = 10/27/16 Pct Recovery = 97% Analysis Date = 10/18/16 Pct Recovery = 97% Analysis Date = 10/18/16 Pct Recovery = 97% Analysis Date = 10/09/16 Pct Recovery = 97% Analysis Date = 10/09/16 Pct Recovery = 97% Analysis Date = 09/29/16 Pct Recovery = 97% Analysis Date = 09/29/16 Pct Recovery = 97% Analysis Date = 09/20/16 Pct Recovery = 97% Analysis Date = 09/20/16 Pct Recovery = 97% Analysis Date = 09/10/16 Pct Recovery = 96% Analysis Date = 09/10/16 Pct Recovery = 96% Analysis Date = 09/01/16 Pct Recovery = 96% Analysis Date = 09/01/16 Pct Recovery = 96% Analysis Date = 08/23/16 Pct Recovery = 96% Analysis Date = 08/23/16 Pct Recovery = 96% Analysis Date = 08/13/16 Pct Recovery = 96% Analysis Date = 08/13/16 Pct Recovery = 96% Analysis Date = 08/04/16 Pct Recovery = 96% Analysis Date = 08/04/16 Pct Recovery = 96% Analysis Date = 07/25/16 Pct Recovery = 96% Analysis Date = 07/25/16 Pct Recovery = 96% Analysis Date = 07/16/16 Pct Recovery = 96% Analysis Date = 07/16/16 Pct Recovery = 96% Analysis Date = 07/07/16 Pct Recovery = 96% Analysis Date = 07/07/16 Pct Recovery = 96% Analysis Date = 06/27/16 Pct Recovery = 95% Analysis Date = 06/27/16 Pct Recovery = 95% Analysis Date = 06/18/16 Pct Recovery = 95% Analysis Date = 06/18/16 Pct Recovery = 95% Analysis Date = 06/08/16 Pct Recovery = 95% Analysis Date = 06/08/16 Pct Recovery = 95% Analysis Date = 05/30/16 Pct Recovery = 95% Analysis Date = 05/30/16 Pct Recovery = 95% Analysis Date = 05/21/16 Pct Recovery = 95% Analysis Date = 05/21/16 Pct Recovery = 95% Analysis Date = 05/11/16 Pct Recovery = 95% Analysis Date = 05/11/16 Pct Recovery = 95% Analysis Date = 05/02/16 Pct Recovery = 95% Analysis Date = 05/02/16 Pct Recovery = 95% Analysis Date = 04/22/16 Pct Recovery = 95% Analysis Date = 04/22/16 Pct Recovery = 95% Analysis Date = 04/13/16 Pct Recovery = 95% Analysis Date = 04/13/16 Pct Recovery = 95% Analysis Date = 04/04/16 Pct Recovery = 94% Analysis Date = 04/04/16 Pct Recovery = 94% Analysis Date = 03/25/16 Pct Recovery = 94% Analysis Date = 03/25/16 Pct Recovery = 94% Analysis Date = 03/16/16 Pct Recovery = 94% Analysis Date = 03/16/16 Pct Recovery = 94% Analysis Date = 03/06/16 Pct Recovery = 94% Analysis Date = 03/06/16 Pct Recovery = 94% Analysis Date = 02/26/16 Pct Recovery = 94% Analysis Date = 02/26/16 Pct Recovery = 94% Analysis Date = 02/17/16 Pct Recovery = 94% Analysis Date = 02/17/16 Pct Recovery = 94% Analysis Date = 02/07/16 Pct Recovery = 94% Analysis Date = 02/07/16 Pct Recovery = 94% Analysis Date = 01/29/16 Pct Recovery = 94% Analysis Date = 01/29/16 Pct Recovery = 94% Analysis Date = 01/19/16 Pct Recovery = 94% Analysis Date = 01/19/16 Pct Recovery = 94% Analysis Date = 01/10/16 Pct Recovery = 94% Analysis Date = 01/10/16 Pct Recovery = 94% Analysis Date = 01/01/16 Pct Recovery = 94% Analysis Date = 01/01/16 Pct Recovery = 94% Analysis Date = 12/22/15 Pct Recovery = 94% Analysis Date = 12/22/15 Pct Recovery = 94% Analysis Date = 12/13/15 Pct Recovery = 93% Analysis Date = 12/13/15 Pct Recovery = 93% Analysis Date = 12/03/15 Pct Recovery = 93% Analysis Date = 12/03/15 Pct Recovery = 93% Analysis Date = 11/24/15 Pct Recovery = 93% Analysis Date = 11/24/15 Pct Recovery = 93% Analysis Date = 11/15/15 Pct Recovery = 93% Analysis Date = 11/15/15 Pct Recovery = 93% Analysis Date = 11/05/15 Pct Recovery = 93% Analysis Date = 11/05/15 Pct Recovery = 93% Analysis Date = 10/27/15 Pct Recovery = 93% Analysis Date = 10/27/15 Pct Recovery = 93% Analysis Date = 10/17/15 Pct Recovery = 93% Analysis Date = 10/17/15 Pct Recovery = 93% Analysis Date = 10/08/15 Pct Recovery = 93% Analysis Date = 10/08/15 Pct Recovery = 93% Analysis Date = 09/29/15 Pct Recovery = 92% Analysis Date = 09/29/15 Pct Recovery = 92% Analysis Date = 09/19/15 Pct Recovery = 92% Analysis Date = 09/19/15 Pct Recovery = 92% Analysis Date = 09/10/15 Pct Recovery = 92% Analysis Date = 09/10/15 Pct Recovery = 92% Analysis Date = 08/31/15 Pct Recovery = 92% Analysis Date = 08/31/15 Pct Recovery = 92% Analysis Date = 08/22/15 Pct Recovery = 92% Analysis Date = 08/22/15 Pct Recovery = 92% Analysis Date = 08/13/15 Pct Recovery = 92% Analysis Date = 08/13/15 Pct Recovery = 92% Analysis Date = 08/03/15 Pct Recovery = 92% Analysis Date = 08/03/15 Pct Recovery = 92% Analysis Date = 07/25/15 Pct Recovery = 92% Analysis Date = 07/25/15 Pct Recovery = 92% Analysis Date = 07/15/15 Pct Recovery = 91% Analysis Date = 07/15/15 Pct Recovery = 91% Analysis Date = 07/06/15 Pct Recovery = 91% Analysis Date = 07/06/15 Pct Recovery = 91% Analysis Date = 06/27/15 Pct Recovery = 91% Analysis Date = 06/27/15 Pct Recovery = 91% Analysis Date = 06/17/15 Pct Recovery = 91% Analysis Date = 06/17/15 Pct Recovery = 91% Analysis Date = 06/08/15 Pct Recovery = 91% Analysis Date = 06/08/15 Pct Recovery = 91% Analysis Date = 05/29/15 Pct Recovery = 91% Analysis Date = 05/29/15 Pct Recovery = 91% Analysis Date = 05/20/15 Pct Recovery = 91% Analysis Date = 05/20/15 Pct Recovery = 91% Analysis Date = 05/11/15 Pct Recovery = 91% Analysis Date = 05/11/15 Pct Recovery = 91% Analysis Date = 05/01/15 Pct Recovery = 90% Analysis Date = 05/01/15 Pct Recovery = 90% Analysis Date = 04/22/15 Pct Recovery = 90% Analysis Date = 04/22/15 Pct Recovery = 90% Analysis Date = 04/12/15 Pct Recovery = 90% Analysis Date = 04/12/15 Pct Recovery = 90% Analysis Date = 04/03/15 Pct Recovery = 90% Analysis Date = 04/03/15 Pct Recovery = 90% Analysis Date = 03/25/15 Pct Recovery = 90% Analysis Date = 03/25/15 Pct Recovery = 90% Analysis Date = 03/15/15 Pct Recovery = 90% Analysis Date = 03/15/15 Pct Recovery = 90% Analysis Date = 03/06/15 Pct Recovery = 90% Analysis Date = 03/06/15 Pct Recovery = 90% Analysis Date = 02/24/15 Pct Recovery = 90% Analysis Date = 02/24/15 Pct Recovery = 90% Analysis Date = 02/15/15 Pct Recovery = 90% Analysis Date = 02/15/15 Pct Recovery = 90% Analysis Date = 02/06/15 Pct Recovery = 90% Analysis Date = 02/06/15 Pct Recovery = 90% Analysis Date = 01/27/15 Pct Recovery = 89% Analysis Date = 01/27/15 Pct Recovery = 89% Analysis Date = 01/18/15 Pct Recovery = 89% Analysis Date = 01/18/15 Pct Recovery = 89% Analysis Date = 01/08/15 Pct Recovery = 89% Analysis Date = 01/08/15 Pct Recovery = 89% Analysis Date = 12/30/14 Pct Recovery = 89% Analysis Date = 12/30/14 Pct Recovery = 89% Analysis Date = 12/21/14 Pct Recovery = 89% Analysis Date = 12/21/14 Pct Recovery = 89% Analysis Date = 12/11/14 Pct Recovery = 89% Analysis Date = 12/11/14 Pct Recovery = 89% Analysis Date = 12/02/14 Pct Recovery = 89% Analysis Date = 12/02/14 Pct Recovery = 89% Analysis Date = 11/22/14 Pct Recovery = 89% Analysis Date = 11/22/14 Pct Recovery = 89% Analysis Date = 11/13/14 Pct Recovery = 89% Analysis Date = 11/13/14 Pct Recovery = 89% Analysis Date = 11/04/14 Pct Recovery = 89% Analysis Date = 11/04/14 Pct Recovery = 89% Analysis Date = 10/25/14 Pct Recovery = 89% Analysis Date = 10/25/14 Pct Recovery = 89% Analysis Date = 10/16/14 Pct Recovery = 88% Analysis Date = 10/16/14 Pct Recovery = 88% Analysis Date = 10/06/14 Pct Recovery = 88% Analysis Date = 10/06/14 Pct Recovery = 88% Analysis Date = 09/27/14 Pct Recovery = 88% Analysis Date = 09/27/14 Pct Recovery = 88% Analysis Date = 09/18/14 Pct Recovery = 88% Analysis Date = 09/18/14 Pct Recovery = 88% Analysis Date = 09/08/14 Pct Recovery = 88% Analysis Date = 09/08/14 Pct Recovery = 88% Analysis Date = 08/30/14 Pct Recovery = 88% Analysis Date = 08/30/14 Pct Recovery = 88% Analysis Date = 08/20/14 Pct Recovery = 88% Analysis Date = 08/20/14 Pct Recovery = 88% Analysis Date = 08/11/14 Pct Recovery = 87% Analysis Date = 08/11/14 Pct Recovery = 87% Analysis Date = 08/02/14 Pct Recovery = 87% Analysis Date = 08/02/14 Pct Recovery = 87% Analysis Date = 07/23/14 Pct Recovery = 87% Analysis Date = 07/23/14 Pct Recovery = 87% Analysis Date = 07/14/14 Pct Recovery = 87% Analysis Date = 07/14/14 Pct Recovery = 87% Analysis Date = 07/04/14 Pct Recovery = 87% Analysis Date = 07/04/14 Pct Recovery = 87% Analysis Date = 06/25/14 Pct Recovery = 87% Analysis Date = 06/25/14 Pct Recovery = 87% Analysis Date = 06/16/14 Pct Recovery = 86% Analysis Date = 06/16/14 Pct Recovery = 86% Analysis Date = 06/06/14 Pct Recovery = 86% Analysis Date = 06/06/14 Pct Recovery = 86% Analysis Date = 05/28/14 Pct Recovery = 86% Analysis Date = 05/28/14 Pct Recovery = 86% Analysis Date = 05/18/14 Pct Recovery = 86% Analysis Date = 05/18/14 Pct Recovery = 86% Analysis Date = 05/09/14 Pct Recovery = 86% Analysis Date = 05/09/14 Pct Recovery = 86% Analysis Date = 04/30/14 Pct Recovery = 85% Analysis Date = 04/30/14 Pct Recovery = 85% Analysis Date = 04/20/14 Pct Recovery = 85% Analysis Date = 04/20/14 Pct Recovery = 85% Analysis Date = 04/11/14 Pct Recovery = 85% Analysis Date = 04/11/14 Pct Recovery = 85% Analysis Date = 04/01/14 Pct Recovery = 84% Analysis Date = 04/01/14 Pct Recovery = 84% Analysis Date = 03/23/14 Pct Recovery = 84% Analysis Date = 03/23/14 Pct Recovery = 84% Analysis Date = 03/14/14 Pct Recovery = 84% Analysis Date = 03/14/14 Pct Recovery = 84% Analysis Date = 03/04/14 Pct Recovery = 84% Analysis Date = 03/04/14 Pct Recovery = 84% Analysis Date = 02/23/14 Pct Recovery = 83% Analysis Date = 02/23/14 Pct Recovery = 83% Analysis Date = 02/13/14 Pct Recovery = 83% Analysis Date = 02/13/14 Pct Recovery = 83% Analysis Date = 02/04/14 Pct Recovery = 83% Analysis Date = 02/04/14 Pct Recovery = 83% Analysis Date = 01/26/14 Pct Recovery = 82% Analysis Date = 01/26/14 Pct Recovery = 82% Analysis Date = 01/16/14 Pct Recovery = 82% Analysis Date = 01/16/14 Pct Recovery = 82% Analysis Date = 01/07/14 Pct Recovery = 82% Analysis Date = 01/07/14 Pct Recovery = 82% Analysis Date = 12/28/13 Pct Recovery = 81% Analysis Date = 12/28/13 Pct Recovery = 81% Analysis Date = 12/19/13 Pct Recovery = 81% Analysis Date = 12/19/13 Pct Recovery = 81% Analysis Date = 12/10/13 Pct Recovery = 81% Analysis Date = 12/10/13 Pct Recovery = 81% Analysis Date = 11/30/13 Pct Recovery = 80% Analysis Date = 11/30/13 Pct Recovery = 80% Analysis Date = 11/21/13 Pct Recovery = 80% Analysis Date = 11/21/13 Pct Recovery = 80% Analysis Date = 11/11/13 Pct Recovery = 80% Analysis Date = 11/11/13 Pct Recovery = 80% Analysis Date = 11/02/13 Pct Recovery = 79% Analysis Date = 11/02/13 Pct Recovery = 79% Analysis Date = 10/24/13 Pct Recovery = 79% Analysis Date = 10/24/13 Pct Recovery = 79% Analysis Date = 10/14/13 Pct Recovery = 79% Analysis Date = 10/14/13 Pct Recovery = 79% Analysis Date = 10/05/13 Pct Recovery = 79% Analysis Date = 10/05/13 Pct Recovery = 79% Analysis Date = 09/25/13 Pct Recovery = 78% Analysis Date = 09/25/13 Pct Recovery = 78% Analysis Date = 09/16/13 Pct Recovery = 78% Analysis Date = 09/16/13 Pct Recovery = 78% Analysis Date = 09/07/13 Pct Recovery = 78% Analysis Date = 09/07/13 Pct Recovery = 78% Analysis Date = 08/28/13 Pct Recovery = 77% Analysis Date = 08/28/13 Pct Recovery = 77% Analysis Date = 08/19/13 Pct Recovery = 77% Analysis Date = 08/19/13 Pct Recovery = 77% Analysis Date = 08/09/13 Pct Recovery = 77% Analysis Date = 08/09/13 Pct Recovery = 77% Analysis Date = 07/31/13 Pct Recovery = 76% Analysis Date = 07/31/13 Pct Recovery = 76% Analysis Date = 07/22/13 Pct Recovery = 76% Analysis Date = 07/22/13 Pct Recovery = 76% Analysis Date = 07/12/13 Pct Recovery = 76% Analysis Date = 07/12/13 Pct Recovery = 76% Analysis Date = 07/03/13 Pct Recovery = 75% Analysis Date = 07/03/13 Pct Recovery = 75% Analysis Date = 06/23/13 Pct Recovery = 75% Analysis Date = 06/23/13 Pct Recovery = 75% Analysis Date = 06/14/13 Pct Recovery = 75% Analysis Date = 06/14/13 Pct Recovery = 75% Analysis Date = 06/05/13 Pct Recovery = 74% Analysis Date = 06/05/13 Pct Recovery = 74% Analysis Date = 05/26/13 Pct Recovery = 74% Analysis Date = 05/26/13 Pct Recovery = 74% Analysis Date = 05/17/13 Pct Recovery = 74% Analysis Date = 05/17/13 Pct Recovery = 74% Analysis Date = 05/07/13 Pct Recovery = 74% Analysis Date = 05/07/13 Pct Recovery = 74% Analysis Date = 04/28/13 Pct Recovery = 73% Analysis Date = 04/28/13 Pct Recovery = 73% Analysis Date = 04/19/13 Pct Recovery = 73% Analysis Date = 04/19/13 Pct Recovery = 73% Analysis Date = 04/09/13 Pct Recovery = 73% Analysis Date = 04/09/13 Pct Recovery = 73% Analysis Date = 03/31/13 Pct Recovery = 72% Analysis Date = 03/31/13 Pct Recovery = 72% Analysis Date = 03/21/13 Pct Recovery = 72% Analysis Date = 03/21/13 Pct Recovery = 72% Analysis Date = 03/12/13 Pct Recovery = 72% Analysis Date = 03/12/13 Pct Recovery = 72% Analysis Date = 03/03/13 Pct Recovery = 71% Analysis Date = 03/03/13 Pct Recovery = 71% Analysis Date = 02/21/13 Pct Recovery = 71% Analysis Date = 02/21/13 Pct Recovery = 71% Analysis Date = 02/12/13 Pct Recovery = 71% Analysis Date = 02/12/13 Pct Recovery = 71% Analysis Date = 02/02/13 Pct Recovery = 70% Analysis Date = 02/02/13 Pct Recovery = 70% Analysis Date = 01/24/13 Pct Recovery = 70% Analysis Date = 01/24/13 Pct Recovery = 70% Analysis Date = 01/15/13 Pct Recovery = 70% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
OXYFLUORFEN

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 79 89% 20% 88% 15%
Total 79 89% 20% 88% 15%

Sample Statistics
OXYFLUORFEN

Characteristic N % % Basis
Plotted 79 100% Spiked
Estimated Values 1 1% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 79 .  
False Negatives 0 0% 0 out of 79
Not Spiked 39 .  
False Positives 0 0% 0 out of 39

OBSP Determination:
PARAOXON-METHYL
METHOD: 2033 , TESTIDCODE: 61664GCM39

Laboratory ID = 20132490342 Lab Value = 0.122 Expected Conc. = 0.175 Report level label = 0.014 Pct Recovery = 70% Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20180390003 Lab Value = 0.079 Expected Conc. = 0.093 Report level label = 0.014 Pct Recovery = 85% Analysis Date = 04/06/18 SpikeMix = Spex Organics EN170808006: 100 µl & Abs 071717Pest: 100 µl SpecificMix = 071717Pest Laboratory ID = 20172510330 Lab Value = 0.079 Expected Conc. = 0.093 Report level label = 0.014 Pct Recovery = 85% Analysis Date = 12/29/17 SpikeMix = ChemService 6537100: 100 µl & Abs 071817Pest: 100 µl SpecificMix = 6537100 Laboratory ID = 20132140002 Lab Value = 0.066 Expected Conc. = 0.088 Report level label = 0.014 Pct Recovery = 75% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl SpecificMix = LB99392 Laboratory ID = 20131370001 Lab Value = 0.081 Expected Conc. = 0.088 Report level label = 0.014 Pct Recovery = 92% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl SpecificMix = LB99392 Laboratory ID = 20163370001 Lab Value = 0.073 Expected Conc. = 0.0878 Report level label = 0.014 Pct Recovery = 83% Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl SpecificMix = B20160331 Laboratory ID = 20163150006 Lab Value = 0.073 Expected Conc. = 0.0878 Report level label = 0.014 Pct Recovery = 83% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl SpecificMix = B20160331 Laboratory ID = 20140370077 Lab Value = 0.067 Expected Conc. = 0.0875 Report level label = 0.014 Pct Recovery = 77% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20132560001 Lab Value = 0.070 Expected Conc. = 0.0875 Report level label = 0.014 Pct Recovery = 80% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20161880109 Lab Value = 0.064 Expected Conc. = 0.085 Report level label = 0.014 Pct Recovery = 76% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl SpecificMix = 03FF076 Laboratory ID = 20152750006 Lab Value = 0.078 Expected Conc. = 0.084 Report level label = 0.014 Pct Recovery = 93% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl SpecificMix = 040615 Laboratory ID = 20152610011 Lab Value = 0.037 Expected Conc. = 0.084 Report level label = 0.014 Pct Recovery = 44% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl SpecificMix = 040615 Laboratory ID = 20172020035 Lab Value = 0.079 Expected Conc. = 0.0712 Report level label = 0.014 Pct Recovery = 111% Analysis Date = 11/07/17 SpikeMix = Abs 071717Pest: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20171720140 Lab Value = 0.057 Expected Conc. = 0.0702 Report level label = 0.014 Pct Recovery = 82% Analysis Date = 08/31/17 SpikeMix = Supelco LC20138V: 80 µl & Phenova B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20171660002 Lab Value = 0.072 Expected Conc. = 0.0702 Report level label = 0.014 Pct Recovery = 103% Analysis Date = 08/23/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20170190026 Lab Value = 0.057 Expected Conc. = 0.0702 Report level label = 0.014 Pct Recovery = 81% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20161470001 Lab Value = 0.065 Expected Conc. = 0.0702 Report level label = 0.014 Pct Recovery = 93% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20170960001 Lab Value = 0.052 Expected Conc. = 0.068 Report level label = 0.014 Pct Recovery = 77% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl SpecificMix = 03FF076 Laboratory ID = 20150720069 Lab Value = 0.019 Expected Conc. = 0.0558 Report level label = 0.014 Pct Recovery = 34% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 03DD006 Laboratory ID = 20143110108 Lab Value = 0.048 Expected Conc. = 0.0558 Report level label = 0.014 Pct Recovery = 86% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 03DD006 Laboratory ID = 20142960086 Lab Value = 0.037 Expected Conc. = 0.0558 Report level label = 0.014 Pct Recovery = 66% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 03DD006 Laboratory ID = 20142720002 Lab Value = 0.047 Expected Conc. = 0.0558 Report level label = 0.014 Pct Recovery = 85% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl SpecificMix = LC06435 Laboratory ID = 20142530087 Lab Value = 0.039 Expected Conc. = 0.0558 Report level label = 0.014 Pct Recovery = 71% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl SpecificMix = LC06435 Laboratory ID = 20142270001 Lab Value = 0.038 Expected Conc. = 0.0558 Report level label = 0.014 Pct Recovery = 68% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl SpecificMix = 03DD006 Laboratory ID = 20141570088 Lab Value = 0.055 Expected Conc. = 0.0558 Report level label = 0.014 Pct Recovery = 98% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl SpecificMix = LC06435 Laboratory ID = 20141220025 Lab Value = 0.062 Expected Conc. = 0.0558 Report level label = 0.014 Pct Recovery = 112% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl SpecificMix = LC06435 Laboratory ID = 20130940097 Lab Value = 0.048 Expected Conc. = 0.051 Report level label = 0.014 Pct Recovery = 94% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = 0507-12-04.2 Laboratory ID = 20123560092 Lab Value = 0.051 Expected Conc. = 0.051 Report level label = 0.014 Pct Recovery = 100% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = 0507-12-04.2 Laboratory ID = 20130810108 Lab Value = 0.046 Expected Conc. = 0.0502 Report level label = 0.014 Pct Recovery = 92% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl SpecificMix = LB92783 Laboratory ID = 20130100066 Lab Value = 0.051 Expected Conc. = 0.0502 Report level label = 0.014 Pct Recovery = 101% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl SpecificMix = LB92783 Laboratory ID = 20173480003 Lab Value = 0.049 Expected Conc. = 0.0465 Report level label = 0.014 Pct Recovery = 105% Analysis Date = 04/05/18 SpikeMix = Abs 071717Pest: 50 µl & ChemService 6567600: 50 µl SpecificMix = 071717Pest Laboratory ID = 20172370001 Lab Value = 0.052 Expected Conc. = 0.0465 Report level label = 0.014 Pct Recovery = 111% Analysis Date = 11/18/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6537100: 50 µl SpecificMix = 6537100 Laboratory ID = 20172230001 Lab Value = 0.055 Expected Conc. = 0.0465 Report level label = 0.014 Pct Recovery = 117% Analysis Date = 10/19/17 SpikeMix = ChemService 6472100: 50 µl & Abs 071717Pest: 50 µl SpecificMix = 071717Pest Laboratory ID = 20161260151 Lab Value = 0.036 Expected Conc. = 0.042 Report level label = 0.014 Pct Recovery = 86% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = EN150513008 Laboratory ID = 20160770090 Lab Value = 0.031 Expected Conc. = 0.042 Report level label = 0.014 Pct Recovery = 75% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = EN150513008 Laboratory ID = 20153510109 Lab Value = 0.026 Expected Conc. = 0.042 Report level label = 0.014 Pct Recovery = 63% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = EN150513008 Laboratory ID = 20152330039 Lab Value = 0.030 Expected Conc. = 0.042 Report level label = 0.014 Pct Recovery = 72% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl SpecificMix = EN150513008 Laboratory ID = 20151900132 Lab Value = 0.049 Expected Conc. = 0.042 Report level label = 0.014 Pct Recovery = 117% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl SpecificMix = 040615 Laboratory ID = 20151550293 Lab Value = 0.041 Expected Conc. = 0.042 Report level label = 0.014 Pct Recovery = 97% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl SpecificMix = 040615 Laboratory ID = 20140510043 Lab Value = 0.024 Expected Conc. = 0.0352 Report level label = 0.014 Pct Recovery = 68% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl SpecificMix = LB99392 Laboratory ID = 20133470008 Lab Value = 0.037 Expected Conc. = 0.0352 Report level label = 0.014 Pct Recovery = 104% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl SpecificMix = LB99392 Laboratory ID = 20133190012 Lab Value = 0.047 Expected Conc. = 0.0352 Report level label = 0.014 Pct Recovery = 134% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = LB99392 Laboratory ID = 20133050050 Lab Value = 0.038 Expected Conc. = 0.0352 Report level label = 0.014 Pct Recovery = 109% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl SpecificMix = LB99392 Laboratory ID = 20171160110 Lab Value = 0.028 Expected Conc. = 0.0351 Report level label = 0.014 Pct Recovery = 80% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = B20160331 Laboratory ID = 20162380004 Lab Value = 0.038 Expected Conc. = 0.0351 Report level label = 0.014 Pct Recovery = 107% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = B20160331 Laboratory ID = 20133580036 Lab Value = 0.029 Expected Conc. = 0.035 Report level label = 0.014 Pct Recovery = 83% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20131790009 Lab Value = 0.034 Expected Conc. = 0.035 Report level label = 0.014 Pct Recovery = 97% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20131510026 Lab Value = 0.037 Expected Conc. = 0.035 Report level label = 0.014 Pct Recovery = 106% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20171510080 Lab Value = 0.030 Expected Conc. = 0.034 Report level label = 0.014 Pct Recovery = 88% Analysis Date = 06/09/17 SpikeMix = Supelco LC20138V: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20170460061 Lab Value = 0.026 Expected Conc. = 0.034 Report level label = 0.014 Pct Recovery = 77% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl SpecificMix = 03FF076 Laboratory ID = 20162660005 Lab Value = 0.025 Expected Conc. = 0.034 Report level label = 0.014 Pct Recovery = 74% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl SpecificMix = 03FF076 Laboratory ID = 20161600087 Lab Value = 0.027 Expected Conc. = 0.034 Report level label = 0.014 Pct Recovery = 81% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20161340228 Lab Value = 0.027 Expected Conc. = 0.034 Report level label = 0.014 Pct Recovery = 80% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl SpecificMix = 03FF076 Laboratory ID = 20161190075 Lab Value = 0.026 Expected Conc. = 0.034 Report level label = 0.014 Pct Recovery = 77% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20180940080 Lab Value = 0.028 Expected Conc. = 0.0279 Report level label = 0.014 Pct Recovery = 100% Analysis Date = 05/31/18 SpikeMix = ChemService 6472100: 30 µl & Abs 071717Pest: 30 µl SpecificMix = 071717Pest Laboratory ID = 20180730064 Lab Value = 0.032 Expected Conc. = 0.0279 Report level label = 0.014 Pct Recovery = 113% Analysis Date = 05/16/18 SpikeMix = Abs 071717Pest: 30 µl & Abs 071817Pest: 30 µl SpecificMix = 071717Pest Laboratory ID = 20173120093 Lab Value = 0.033 Expected Conc. = 0.0279 Report level label = 0.014 Pct Recovery = 119% Analysis Date = 03/10/18 SpikeMix = ChemService 6472100: 30 µl & ChemService 6537100: 30 µl SpecificMix = 6537100 Laboratory ID = 20150150115 Lab Value = 0.033 Expected Conc. = 0.0279 Report level label = 0.014 Pct Recovery = 117% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl SpecificMix = LC06435 Laboratory ID = 20143370094 Lab Value = 0.024 Expected Conc. = 0.0279 Report level label = 0.014 Pct Recovery = 86% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl SpecificMix = LC06435 Laboratory ID = 20142200164 Lab Value = 0.019 Expected Conc. = 0.0279 Report level label = 0.014 Pct Recovery = 68% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 03DD006 Laboratory ID = 20141910243 Lab Value = 0.019 Expected Conc. = 0.0279 Report level label = 0.014 Pct Recovery = 67% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = LC06435 Laboratory ID = 20141840097 Lab Value = 0.019 Expected Conc. = 0.0279 Report level label = 0.014 Pct Recovery = 70% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl SpecificMix = LC06435 Laboratory ID = 20141640076 Lab Value = 0.020 Expected Conc. = 0.0279 Report level label = 0.014 Pct Recovery = 72% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = 03DD006 Laboratory ID = 20141420140 Lab Value = 0.016 Expected Conc. = 0.0279 Report level label = 0.014 Pct Recovery = 59% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 03DD006 Laboratory ID = 20141080004 Lab Value = 0.023 Expected Conc. = 0.0279 Report level label = 0.014 Pct Recovery = 82% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl SpecificMix = 03DD006 Laboratory ID = 20161050143 Lab Value = 0.024 Expected Conc. = 0.021 Report level label = 0.014 Pct Recovery = 114% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Laboratory ID = 20160430111 Lab Value = 0.023 Expected Conc. = 0.021 Report level label = 0.014 Pct Recovery = 109% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Laboratory ID = 20160560044 Lab Value = 0.019 Expected Conc. = 0.021 Report level label = 0.014 Pct Recovery = 90% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl SpecificMix = EN150513008 Laboratory ID = 20160070059 Lab Value = 0.016 Expected Conc. = 0.021 Report level label = 0.014 Pct Recovery = 75% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = 040615 Laboratory ID = 20153030068 Lab Value = 0.018 Expected Conc. = 0.021 Report level label = 0.014 Pct Recovery = 85% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150513008 Laboratory ID = 20152190003 Lab Value = 0.019 Expected Conc. = 0.021 Report level label = 0.014 Pct Recovery = 91% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150513008 Laboratory ID = 20151480170 Lab Value = 0.022 Expected Conc. = 0.021 Report level label = 0.014 Pct Recovery = 106% Analysis Date = 06/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150513008 Laboratory ID = 20151380009 Lab Value = 0.028 Expected Conc. = 0.021 Report level label = 0.014 Pct Recovery = 131% Analysis Date = 05/30/15 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Laboratory ID = 20151210037 Lab Value = 0.021 Expected Conc. = 0.021 Report level label = 0.014 Pct Recovery = 98% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Laboratory ID = 20130510051 Lab Value = 0.030 Expected Conc. = 0.0204 Report level label = 0.014 Pct Recovery = 147% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl SpecificMix = 0507-12-04.2 Laboratory ID = 20130390105 Lab Value = 0.018 Expected Conc. = 0.0201 Report level label = 0.014 Pct Recovery = 92% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl SpecificMix = LB92783 Analysis Date = 05/31/18 Pct Recovery = 103% Analysis Date = 05/21/18 Pct Recovery = 102% Analysis Date = 05/21/18 Pct Recovery = 102% Analysis Date = 05/11/18 Pct Recovery = 102% Analysis Date = 05/11/18 Pct Recovery = 102% Analysis Date = 05/01/18 Pct Recovery = 102% Analysis Date = 05/01/18 Pct Recovery = 102% Analysis Date = 04/21/18 Pct Recovery = 102% Analysis Date = 04/21/18 Pct Recovery = 102% Analysis Date = 04/11/18 Pct Recovery = 101% Analysis Date = 04/11/18 Pct Recovery = 101% Analysis Date = 04/02/18 Pct Recovery = 101% Analysis Date = 04/02/18 Pct Recovery = 101% Analysis Date = 03/23/18 Pct Recovery = 101% Analysis Date = 03/23/18 Pct Recovery = 101% Analysis Date = 03/13/18 Pct Recovery = 100% Analysis Date = 03/13/18 Pct Recovery = 100% Analysis Date = 03/03/18 Pct Recovery = 100% Analysis Date = 03/03/18 Pct Recovery = 100% Analysis Date = 02/21/18 Pct Recovery = 100% Analysis Date = 02/21/18 Pct Recovery = 100% Analysis Date = 02/12/18 Pct Recovery = 100% Analysis Date = 02/12/18 Pct Recovery = 100% Analysis Date = 02/02/18 Pct Recovery = 99% Analysis Date = 02/02/18 Pct Recovery = 99% Analysis Date = 01/23/18 Pct Recovery = 99% Analysis Date = 01/23/18 Pct Recovery = 99% Analysis Date = 01/13/18 Pct Recovery = 99% Analysis Date = 01/13/18 Pct Recovery = 99% Analysis Date = 01/03/18 Pct Recovery = 99% Analysis Date = 01/03/18 Pct Recovery = 99% Analysis Date = 12/25/17 Pct Recovery = 98% Analysis Date = 12/25/17 Pct Recovery = 98% Analysis Date = 12/15/17 Pct Recovery = 98% Analysis Date = 12/15/17 Pct Recovery = 98% Analysis Date = 12/05/17 Pct Recovery = 98% Analysis Date = 12/05/17 Pct Recovery = 98% Analysis Date = 11/25/17 Pct Recovery = 98% Analysis Date = 11/25/17 Pct Recovery = 98% Analysis Date = 11/15/17 Pct Recovery = 97% Analysis Date = 11/15/17 Pct Recovery = 97% Analysis Date = 11/05/17 Pct Recovery = 97% Analysis Date = 11/05/17 Pct Recovery = 97% Analysis Date = 10/27/17 Pct Recovery = 97% Analysis Date = 10/27/17 Pct Recovery = 97% Analysis Date = 10/17/17 Pct Recovery = 96% Analysis Date = 10/17/17 Pct Recovery = 96% Analysis Date = 10/07/17 Pct Recovery = 96% Analysis Date = 10/07/17 Pct Recovery = 96% Analysis Date = 09/27/17 Pct Recovery = 96% Analysis Date = 09/27/17 Pct Recovery = 96% Analysis Date = 09/17/17 Pct Recovery = 96% Analysis Date = 09/17/17 Pct Recovery = 96% Analysis Date = 09/08/17 Pct Recovery = 95% Analysis Date = 09/08/17 Pct Recovery = 95% Analysis Date = 08/29/17 Pct Recovery = 95% Analysis Date = 08/29/17 Pct Recovery = 95% Analysis Date = 08/19/17 Pct Recovery = 95% Analysis Date = 08/19/17 Pct Recovery = 95% Analysis Date = 08/09/17 Pct Recovery = 95% Analysis Date = 08/09/17 Pct Recovery = 95% Analysis Date = 07/30/17 Pct Recovery = 94% Analysis Date = 07/30/17 Pct Recovery = 94% Analysis Date = 07/21/17 Pct Recovery = 94% Analysis Date = 07/21/17 Pct Recovery = 94% Analysis Date = 07/11/17 Pct Recovery = 94% Analysis Date = 07/11/17 Pct Recovery = 94% Analysis Date = 07/01/17 Pct Recovery = 94% Analysis Date = 07/01/17 Pct Recovery = 94% Analysis Date = 06/21/17 Pct Recovery = 93% Analysis Date = 06/21/17 Pct Recovery = 93% Analysis Date = 06/11/17 Pct Recovery = 93% Analysis Date = 06/11/17 Pct Recovery = 93% Analysis Date = 06/02/17 Pct Recovery = 93% Analysis Date = 06/02/17 Pct Recovery = 93% Analysis Date = 05/23/17 Pct Recovery = 93% Analysis Date = 05/23/17 Pct Recovery = 93% Analysis Date = 05/13/17 Pct Recovery = 92% Analysis Date = 05/13/17 Pct Recovery = 92% Analysis Date = 05/03/17 Pct Recovery = 92% Analysis Date = 05/03/17 Pct Recovery = 92% Analysis Date = 04/23/17 Pct Recovery = 92% Analysis Date = 04/23/17 Pct Recovery = 92% Analysis Date = 04/13/17 Pct Recovery = 92% Analysis Date = 04/13/17 Pct Recovery = 92% Analysis Date = 04/04/17 Pct Recovery = 92% Analysis Date = 04/04/17 Pct Recovery = 92% Analysis Date = 03/25/17 Pct Recovery = 91% Analysis Date = 03/25/17 Pct Recovery = 91% Analysis Date = 03/15/17 Pct Recovery = 91% Analysis Date = 03/15/17 Pct Recovery = 91% Analysis Date = 03/05/17 Pct Recovery = 91% Analysis Date = 03/05/17 Pct Recovery = 91% Analysis Date = 02/23/17 Pct Recovery = 91% Analysis Date = 02/23/17 Pct Recovery = 91% Analysis Date = 02/14/17 Pct Recovery = 90% Analysis Date = 02/14/17 Pct Recovery = 90% Analysis Date = 02/04/17 Pct Recovery = 90% Analysis Date = 02/04/17 Pct Recovery = 90% Analysis Date = 01/25/17 Pct Recovery = 90% Analysis Date = 01/25/17 Pct Recovery = 90% Analysis Date = 01/15/17 Pct Recovery = 90% Analysis Date = 01/15/17 Pct Recovery = 90% Analysis Date = 01/05/17 Pct Recovery = 89% Analysis Date = 01/05/17 Pct Recovery = 89% Analysis Date = 12/27/16 Pct Recovery = 89% Analysis Date = 12/27/16 Pct Recovery = 89% Analysis Date = 12/17/16 Pct Recovery = 89% Analysis Date = 12/17/16 Pct Recovery = 89% Analysis Date = 12/07/16 Pct Recovery = 89% Analysis Date = 12/07/16 Pct Recovery = 89% Analysis Date = 11/27/16 Pct Recovery = 89% Analysis Date = 11/27/16 Pct Recovery = 89% Analysis Date = 11/17/16 Pct Recovery = 89% Analysis Date = 11/17/16 Pct Recovery = 89% Analysis Date = 11/08/16 Pct Recovery = 88% Analysis Date = 11/08/16 Pct Recovery = 88% Analysis Date = 10/29/16 Pct Recovery = 88% Analysis Date = 10/29/16 Pct Recovery = 88% Analysis Date = 10/19/16 Pct Recovery = 88% Analysis Date = 10/19/16 Pct Recovery = 88% Analysis Date = 10/09/16 Pct Recovery = 88% Analysis Date = 10/09/16 Pct Recovery = 88% Analysis Date = 09/29/16 Pct Recovery = 88% Analysis Date = 09/29/16 Pct Recovery = 88% Analysis Date = 09/19/16 Pct Recovery = 88% Analysis Date = 09/19/16 Pct Recovery = 88% Analysis Date = 09/10/16 Pct Recovery = 88% Analysis Date = 09/10/16 Pct Recovery = 88% Analysis Date = 08/31/16 Pct Recovery = 88% Analysis Date = 08/31/16 Pct Recovery = 88% Analysis Date = 08/21/16 Pct Recovery = 88% Analysis Date = 08/21/16 Pct Recovery = 88% Analysis Date = 08/11/16 Pct Recovery = 87% Analysis Date = 08/11/16 Pct Recovery = 87% Analysis Date = 08/01/16 Pct Recovery = 87% Analysis Date = 08/01/16 Pct Recovery = 87% Analysis Date = 07/23/16 Pct Recovery = 87% Analysis Date = 07/23/16 Pct Recovery = 87% Analysis Date = 07/13/16 Pct Recovery = 87% Analysis Date = 07/13/16 Pct Recovery = 87% Analysis Date = 07/03/16 Pct Recovery = 87% Analysis Date = 07/03/16 Pct Recovery = 87% Analysis Date = 06/23/16 Pct Recovery = 87% Analysis Date = 06/23/16 Pct Recovery = 87% Analysis Date = 06/13/16 Pct Recovery = 87% Analysis Date = 06/13/16 Pct Recovery = 87% Analysis Date = 06/04/16 Pct Recovery = 87% Analysis Date = 06/04/16 Pct Recovery = 87% Analysis Date = 05/25/16 Pct Recovery = 87% Analysis Date = 05/25/16 Pct Recovery = 87% Analysis Date = 05/15/16 Pct Recovery = 86% Analysis Date = 05/15/16 Pct Recovery = 86% Analysis Date = 05/05/16 Pct Recovery = 86% Analysis Date = 05/05/16 Pct Recovery = 86% Analysis Date = 04/25/16 Pct Recovery = 86% Analysis Date = 04/25/16 Pct Recovery = 86% Analysis Date = 04/16/16 Pct Recovery = 86% Analysis Date = 04/16/16 Pct Recovery = 86% Analysis Date = 04/06/16 Pct Recovery = 86% Analysis Date = 04/06/16 Pct Recovery = 86% Analysis Date = 03/27/16 Pct Recovery = 86% Analysis Date = 03/27/16 Pct Recovery = 86% Analysis Date = 03/17/16 Pct Recovery = 86% Analysis Date = 03/17/16 Pct Recovery = 86% Analysis Date = 03/07/16 Pct Recovery = 86% Analysis Date = 03/07/16 Pct Recovery = 86% Analysis Date = 02/26/16 Pct Recovery = 86% Analysis Date = 02/26/16 Pct Recovery = 86% Analysis Date = 02/17/16 Pct Recovery = 86% Analysis Date = 02/17/16 Pct Recovery = 86% Analysis Date = 02/07/16 Pct Recovery = 87% Analysis Date = 02/07/16 Pct Recovery = 87% Analysis Date = 01/28/16 Pct Recovery = 87% Analysis Date = 01/28/16 Pct Recovery = 87% Analysis Date = 01/18/16 Pct Recovery = 87% Analysis Date = 01/18/16 Pct Recovery = 87% Analysis Date = 01/08/16 Pct Recovery = 87% Analysis Date = 01/08/16 Pct Recovery = 87% Analysis Date = 12/30/15 Pct Recovery = 87% Analysis Date = 12/30/15 Pct Recovery = 87% Analysis Date = 12/20/15 Pct Recovery = 86% Analysis Date = 12/20/15 Pct Recovery = 86% Analysis Date = 12/10/15 Pct Recovery = 86% Analysis Date = 12/10/15 Pct Recovery = 86% Analysis Date = 11/30/15 Pct Recovery = 86% Analysis Date = 11/30/15 Pct Recovery = 86% Analysis Date = 11/20/15 Pct Recovery = 86% Analysis Date = 11/20/15 Pct Recovery = 86% Analysis Date = 11/11/15 Pct Recovery = 86% Analysis Date = 11/11/15 Pct Recovery = 86% Analysis Date = 11/01/15 Pct Recovery = 86% Analysis Date = 11/01/15 Pct Recovery = 86% Analysis Date = 10/22/15 Pct Recovery = 86% Analysis Date = 10/22/15 Pct Recovery = 86% Analysis Date = 10/12/15 Pct Recovery = 86% Analysis Date = 10/12/15 Pct Recovery = 86% Analysis Date = 10/02/15 Pct Recovery = 86% Analysis Date = 10/02/15 Pct Recovery = 86% Analysis Date = 09/23/15 Pct Recovery = 86% Analysis Date = 09/23/15 Pct Recovery = 86% Analysis Date = 09/13/15 Pct Recovery = 86% Analysis Date = 09/13/15 Pct Recovery = 86% Analysis Date = 09/03/15 Pct Recovery = 85% Analysis Date = 09/03/15 Pct Recovery = 85% Analysis Date = 08/24/15 Pct Recovery = 85% Analysis Date = 08/24/15 Pct Recovery = 85% Analysis Date = 08/14/15 Pct Recovery = 85% Analysis Date = 08/14/15 Pct Recovery = 85% Analysis Date = 08/04/15 Pct Recovery = 85% Analysis Date = 08/04/15 Pct Recovery = 85% Analysis Date = 07/26/15 Pct Recovery = 85% Analysis Date = 07/26/15 Pct Recovery = 85% Analysis Date = 07/16/15 Pct Recovery = 85% Analysis Date = 07/16/15 Pct Recovery = 85% Analysis Date = 07/06/15 Pct Recovery = 85% Analysis Date = 07/06/15 Pct Recovery = 85% Analysis Date = 06/26/15 Pct Recovery = 85% Analysis Date = 06/26/15 Pct Recovery = 85% Analysis Date = 06/16/15 Pct Recovery = 85% Analysis Date = 06/16/15 Pct Recovery = 85% Analysis Date = 06/07/15 Pct Recovery = 85% Analysis Date = 06/07/15 Pct Recovery = 85% Analysis Date = 05/28/15 Pct Recovery = 85% Analysis Date = 05/28/15 Pct Recovery = 85% Analysis Date = 05/18/15 Pct Recovery = 85% Analysis Date = 05/18/15 Pct Recovery = 85% Analysis Date = 05/08/15 Pct Recovery = 85% Analysis Date = 05/08/15 Pct Recovery = 85% Analysis Date = 04/28/15 Pct Recovery = 85% Analysis Date = 04/28/15 Pct Recovery = 85% Analysis Date = 04/19/15 Pct Recovery = 85% Analysis Date = 04/19/15 Pct Recovery = 85% Analysis Date = 04/09/15 Pct Recovery = 85% Analysis Date = 04/09/15 Pct Recovery = 85% Analysis Date = 03/30/15 Pct Recovery = 85% Analysis Date = 03/30/15 Pct Recovery = 85% Analysis Date = 03/20/15 Pct Recovery = 85% Analysis Date = 03/20/15 Pct Recovery = 85% Analysis Date = 03/10/15 Pct Recovery = 85% Analysis Date = 03/10/15 Pct Recovery = 85% Analysis Date = 02/28/15 Pct Recovery = 85% Analysis Date = 02/28/15 Pct Recovery = 85% Analysis Date = 02/19/15 Pct Recovery = 85% Analysis Date = 02/19/15 Pct Recovery = 85% Analysis Date = 02/09/15 Pct Recovery = 85% Analysis Date = 02/09/15 Pct Recovery = 85% Analysis Date = 01/30/15 Pct Recovery = 85% Analysis Date = 01/30/15 Pct Recovery = 85% Analysis Date = 01/20/15 Pct Recovery = 85% Analysis Date = 01/20/15 Pct Recovery = 85% Analysis Date = 01/10/15 Pct Recovery = 84% Analysis Date = 01/10/15 Pct Recovery = 84% Analysis Date = 01/01/15 Pct Recovery = 84% Analysis Date = 01/01/15 Pct Recovery = 84% Analysis Date = 12/22/14 Pct Recovery = 84% Analysis Date = 12/22/14 Pct Recovery = 84% Analysis Date = 12/12/14 Pct Recovery = 84% Analysis Date = 12/12/14 Pct Recovery = 84% Analysis Date = 12/02/14 Pct Recovery = 84% Analysis Date = 12/02/14 Pct Recovery = 84% Analysis Date = 11/22/14 Pct Recovery = 84% Analysis Date = 11/22/14 Pct Recovery = 84% Analysis Date = 11/13/14 Pct Recovery = 84% Analysis Date = 11/13/14 Pct Recovery = 84% Analysis Date = 11/03/14 Pct Recovery = 84% Analysis Date = 11/03/14 Pct Recovery = 84% Analysis Date = 10/24/14 Pct Recovery = 84% Analysis Date = 10/24/14 Pct Recovery = 84% Analysis Date = 10/14/14 Pct Recovery = 84% Analysis Date = 10/14/14 Pct Recovery = 84% Analysis Date = 10/04/14 Pct Recovery = 84% Analysis Date = 10/04/14 Pct Recovery = 84% Analysis Date = 09/25/14 Pct Recovery = 84% Analysis Date = 09/25/14 Pct Recovery = 84% Analysis Date = 09/15/14 Pct Recovery = 84% Analysis Date = 09/15/14 Pct Recovery = 84% Analysis Date = 09/05/14 Pct Recovery = 85% Analysis Date = 09/05/14 Pct Recovery = 85% Analysis Date = 08/26/14 Pct Recovery = 85% Analysis Date = 08/26/14 Pct Recovery = 85% Analysis Date = 08/16/14 Pct Recovery = 85% Analysis Date = 08/16/14 Pct Recovery = 85% Analysis Date = 08/06/14 Pct Recovery = 85% Analysis Date = 08/06/14 Pct Recovery = 85% Analysis Date = 07/28/14 Pct Recovery = 85% Analysis Date = 07/28/14 Pct Recovery = 85% Analysis Date = 07/18/14 Pct Recovery = 85% Analysis Date = 07/18/14 Pct Recovery = 85% Analysis Date = 07/08/14 Pct Recovery = 85% Analysis Date = 07/08/14 Pct Recovery = 85% Analysis Date = 06/28/14 Pct Recovery = 85% Analysis Date = 06/28/14 Pct Recovery = 85% Analysis Date = 06/18/14 Pct Recovery = 85% Analysis Date = 06/18/14 Pct Recovery = 85% Analysis Date = 06/09/14 Pct Recovery = 86% Analysis Date = 06/09/14 Pct Recovery = 86% Analysis Date = 05/30/14 Pct Recovery = 86% Analysis Date = 05/30/14 Pct Recovery = 86% Analysis Date = 05/20/14 Pct Recovery = 86% Analysis Date = 05/20/14 Pct Recovery = 86% Analysis Date = 05/10/14 Pct Recovery = 86% Analysis Date = 05/10/14 Pct Recovery = 86% Analysis Date = 04/30/14 Pct Recovery = 87% Analysis Date = 04/30/14 Pct Recovery = 87% Analysis Date = 04/21/14 Pct Recovery = 87% Analysis Date = 04/21/14 Pct Recovery = 87% Analysis Date = 04/11/14 Pct Recovery = 87% Analysis Date = 04/11/14 Pct Recovery = 87% Analysis Date = 04/01/14 Pct Recovery = 87% Analysis Date = 04/01/14 Pct Recovery = 87% Analysis Date = 03/22/14 Pct Recovery = 88% Analysis Date = 03/22/14 Pct Recovery = 88% Analysis Date = 03/12/14 Pct Recovery = 88% Analysis Date = 03/12/14 Pct Recovery = 88% Analysis Date = 03/03/14 Pct Recovery = 88% Analysis Date = 03/03/14 Pct Recovery = 88% Analysis Date = 02/21/14 Pct Recovery = 89% Analysis Date = 02/21/14 Pct Recovery = 89% Analysis Date = 02/11/14 Pct Recovery = 89% Analysis Date = 02/11/14 Pct Recovery = 89% Analysis Date = 02/01/14 Pct Recovery = 89% Analysis Date = 02/01/14 Pct Recovery = 89% Analysis Date = 01/22/14 Pct Recovery = 89% Analysis Date = 01/22/14 Pct Recovery = 89% Analysis Date = 01/12/14 Pct Recovery = 90% Analysis Date = 01/12/14 Pct Recovery = 90% Analysis Date = 01/03/14 Pct Recovery = 90% Analysis Date = 01/03/14 Pct Recovery = 90% Analysis Date = 12/24/13 Pct Recovery = 90% Analysis Date = 12/24/13 Pct Recovery = 90% Analysis Date = 12/14/13 Pct Recovery = 91% Analysis Date = 12/14/13 Pct Recovery = 91% Analysis Date = 12/04/13 Pct Recovery = 91% Analysis Date = 12/04/13 Pct Recovery = 91% Analysis Date = 11/24/13 Pct Recovery = 91% Analysis Date = 11/24/13 Pct Recovery = 91% Analysis Date = 11/15/13 Pct Recovery = 92% Analysis Date = 11/15/13 Pct Recovery = 92% Analysis Date = 11/05/13 Pct Recovery = 92% Analysis Date = 11/05/13 Pct Recovery = 92% Analysis Date = 10/26/13 Pct Recovery = 92% Analysis Date = 10/26/13 Pct Recovery = 92% Analysis Date = 10/16/13 Pct Recovery = 92% Analysis Date = 10/16/13 Pct Recovery = 92% Analysis Date = 10/06/13 Pct Recovery = 93% Analysis Date = 10/06/13 Pct Recovery = 93% Analysis Date = 09/27/13 Pct Recovery = 93% Analysis Date = 09/27/13 Pct Recovery = 93% Analysis Date = 09/17/13 Pct Recovery = 93% Analysis Date = 09/17/13 Pct Recovery = 93% Analysis Date = 09/07/13 Pct Recovery = 94% Analysis Date = 09/07/13 Pct Recovery = 94% Analysis Date = 08/28/13 Pct Recovery = 94% Analysis Date = 08/28/13 Pct Recovery = 94% Analysis Date = 08/18/13 Pct Recovery = 94% Analysis Date = 08/18/13 Pct Recovery = 94% Analysis Date = 08/09/13 Pct Recovery = 94% Analysis Date = 08/09/13 Pct Recovery = 94% Analysis Date = 07/30/13 Pct Recovery = 95% Analysis Date = 07/30/13 Pct Recovery = 95% Analysis Date = 07/20/13 Pct Recovery = 95% Analysis Date = 07/20/13 Pct Recovery = 95% Analysis Date = 07/10/13 Pct Recovery = 95% Analysis Date = 07/10/13 Pct Recovery = 95% Analysis Date = 06/30/13 Pct Recovery = 96% Analysis Date = 06/30/13 Pct Recovery = 96% Analysis Date = 06/20/13 Pct Recovery = 96% Analysis Date = 06/20/13 Pct Recovery = 96% Analysis Date = 06/11/13 Pct Recovery = 97% Analysis Date = 06/11/13 Pct Recovery = 97% Analysis Date = 06/01/13 Pct Recovery = 97% Analysis Date = 06/01/13 Pct Recovery = 97% Analysis Date = 05/22/13 Pct Recovery = 97% Analysis Date = 05/22/13 Pct Recovery = 97% Analysis Date = 05/12/13 Pct Recovery = 98% Analysis Date = 05/12/13 Pct Recovery = 98% Analysis Date = 05/02/13 Pct Recovery = 98% Analysis Date = 05/02/13 Pct Recovery = 98% Analysis Date = 04/23/13 Pct Recovery = 98% Analysis Date = 04/23/13 Pct Recovery = 98% Analysis Date = 04/13/13 Pct Recovery = 99% Analysis Date = 04/13/13 Pct Recovery = 99% Analysis Date = 04/03/13 Pct Recovery = 99% Analysis Date = 04/03/13 Pct Recovery = 99% Analysis Date = 03/24/13 Pct Recovery = 99% Analysis Date = 03/24/13 Pct Recovery = 99% Analysis Date = 03/14/13 Pct Recovery = 100% Analysis Date = 03/14/13 Pct Recovery = 100% Analysis Date = 03/05/13 Pct Recovery = 100% Analysis Date = 03/05/13 Pct Recovery = 100% Analysis Date = 02/23/13 Pct Recovery = 100% Analysis Date = 02/23/13 Pct Recovery = 100% Analysis Date = 02/13/13 Pct Recovery = 101% Analysis Date = 02/13/13 Pct Recovery = 101% Analysis Date = 02/03/13 Pct Recovery = 101% Analysis Date = 02/03/13 Pct Recovery = 101% Analysis Date = 01/24/13 Pct Recovery = 101% Analysis Date = 01/24/13 Pct Recovery = 101% Analysis Date = 01/15/13 Pct Recovery = 102% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
PARAOXON-METHYL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 76 89% 20% 86% 20%
Total 76 89% 20% 86% 20%

Sample Statistics
PARAOXON-METHYL

Characteristic N % % Basis
Plotted 76 96% Spiked
Estimated Values 76 96% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 79 .  
False Negatives 3 4% 3 out of 79
Not Spiked 55 .  
False Positives 0 0% 0 out of 55

OBSP Determination:
PARATHION-METHYL
METHOD: 2033 , TESTIDCODE: 82667GCM35

Laboratory ID = 20142530087 Lab Value = 0.072 Expected Conc. = 0.0319 Report level label = 0.008 Pct Recovery = 225% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl SpecificMix = LC06435 Laboratory ID = 20142960086 Lab Value = 0.079 Expected Conc. = 0.0318 Report level label = 0.008 Pct Recovery = 247% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 03DD006 Laboratory ID = 20143370094 Lab Value = 0.049 Expected Conc. = 0.016 Report level label = 0.008 Pct Recovery = 309% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl SpecificMix = LC06435 Laboratory ID = 20142200164 Lab Value = 0.049 Expected Conc. = 0.0159 Report level label = 0.008 Pct Recovery = 308% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 03DD006 Laboratory ID = 20140100085 Lab Value = 0.090 Expected Conc. = 0.11 Report level label = 0.008 Pct Recovery = 82% Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl SpecificMix = T1130514013 Laboratory ID = 20132490342 Lab Value = 0.083 Expected Conc. = 0.11 Report level label = 0.008 Pct Recovery = 75% Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl SpecificMix = T1130514013 Laboratory ID = 20130250061 Lab Value = 0.079 Expected Conc. = 0.1 Report level label = 0.008 Pct Recovery = 79% Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl SpecificMix = A088380 Laboratory ID = 20131370001 Lab Value = 0.065 Expected Conc. = 0.0555 Report level label = 0.008 Pct Recovery = 117% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl SpecificMix = 1473000 Laboratory ID = 20140370077 Lab Value = 0.042 Expected Conc. = 0.055 Report level label = 0.008 Pct Recovery = 75% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl SpecificMix = T1130514013 Laboratory ID = 20132690010 Lab Value = 0.053 Expected Conc. = 0.055 Report level label = 0.008 Pct Recovery = 97% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl SpecificMix = T1130514013 Laboratory ID = 20172510330 Lab Value = 0.053 Expected Conc. = 0.053 Report level label = 0.008 Pct Recovery = 101% Analysis Date = 12/29/17 SpikeMix = ChemService 6537100: 100 µl & Abs 071817Pest: 100 µl SpecificMix = 6537100 Laboratory ID = 20163370001 Lab Value = 0.056 Expected Conc. = 0.0503 Report level label = 0.008 Pct Recovery = 111% Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl SpecificMix = LC20138V Laboratory ID = 20162860079 Lab Value = 0.047 Expected Conc. = 0.05 Report level label = 0.008 Pct Recovery = 94% Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl SpecificMix = 5054800 Laboratory ID = 20161880109 Lab Value = 0.066 Expected Conc. = 0.05 Report level label = 0.008 Pct Recovery = 133% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl SpecificMix = 5054800 Laboratory ID = 20140230082 Lab Value = 0.045 Expected Conc. = 0.05 Report level label = 0.008 Pct Recovery = 91% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl SpecificMix = A093651 Laboratory ID = 20132420001 Lab Value = 0.045 Expected Conc. = 0.05 Report level label = 0.008 Pct Recovery = 90% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl SpecificMix = A093651 Laboratory ID = 20130810108 Lab Value = 0.048 Expected Conc. = 0.05 Report level label = 0.008 Pct Recovery = 95% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl SpecificMix = T1120530013 Laboratory ID = 20123560092 Lab Value = 0.051 Expected Conc. = 0.05 Report level label = 0.008 Pct Recovery = 102% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = T1120530013 Laboratory ID = 20152750006 Lab Value = 0.050 Expected Conc. = 0.048 Report level label = 0.008 Pct Recovery = 104% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl SpecificMix = EN150514012 Laboratory ID = 20152460215 Lab Value = 0.038 Expected Conc. = 0.048 Report level label = 0.008 Pct Recovery = 79% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl SpecificMix = EN150514012 Laboratory ID = 20171720140 Lab Value = 0.046 Expected Conc. = 0.0402 Report level label = 0.008 Pct Recovery = 115% Analysis Date = 08/31/17 SpikeMix = Supelco LC20138V: 80 µl & Phenova B20160331: 80 µl SpecificMix = LC20138V Laboratory ID = 20170740063 Lab Value = 0.041 Expected Conc. = 0.0402 Report level label = 0.008 Pct Recovery = 101% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl SpecificMix = LC20138V Laboratory ID = 20161470001 Lab Value = 0.049 Expected Conc. = 0.0402 Report level label = 0.008 Pct Recovery = 123% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl SpecificMix = LC20138V Laboratory ID = 20171380001 Lab Value = 0.038 Expected Conc. = 0.04 Report level label = 0.008 Pct Recovery = 95% Analysis Date = 06/07/17 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 5054800 Laboratory ID = 20170960001 Lab Value = 0.042 Expected Conc. = 0.04 Report level label = 0.008 Pct Recovery = 105% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl SpecificMix = 5054800 Laboratory ID = 20161740258 Lab Value = 0.036 Expected Conc. = 0.04 Report level label = 0.008 Pct Recovery = 90% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 5054800 Laboratory ID = 20142720002 Lab Value = 0.030 Expected Conc. = 0.0319 Report level label = 0.008 Pct Recovery = 93% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl SpecificMix = LC06435 Laboratory ID = 20141570088 Lab Value = 0.035 Expected Conc. = 0.0319 Report level label = 0.008 Pct Recovery = 108% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl SpecificMix = LC06435 Laboratory ID = 20141220025 Lab Value = 0.037 Expected Conc. = 0.0319 Report level label = 0.008 Pct Recovery = 117% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl SpecificMix = LC06435 Laboratory ID = 20150720069 Lab Value = 0.034 Expected Conc. = 0.0318 Report level label = 0.008 Pct Recovery = 107% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 03DD006 Laboratory ID = 20143110108 Lab Value = 0.034 Expected Conc. = 0.0318 Report level label = 0.008 Pct Recovery = 108% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 03DD006 Laboratory ID = 20142270001 Lab Value = 0.028 Expected Conc. = 0.0318 Report level label = 0.008 Pct Recovery = 86% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl SpecificMix = 03DD006 Laboratory ID = 20172370001 Lab Value = 0.033 Expected Conc. = 0.0265 Report level label = 0.008 Pct Recovery = 125% Analysis Date = 11/18/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6537100: 50 µl SpecificMix = 6537100 Laboratory ID = 20172230001 Lab Value = 0.036 Expected Conc. = 0.0265 Report level label = 0.008 Pct Recovery = 134% Analysis Date = 10/19/17 SpikeMix = ChemService 6472100: 50 µl & Abs 071717Pest: 50 µl SpecificMix = 071717Pest Laboratory ID = 20160630046 Lab Value = 0.023 Expected Conc. = 0.024 Report level label = 0.008 Pct Recovery = 96% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = EN150514012 Laboratory ID = 20153440001 Lab Value = 0.019 Expected Conc. = 0.024 Report level label = 0.008 Pct Recovery = 80% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = EN150514012 Laboratory ID = 20152330039 Lab Value = 0.020 Expected Conc. = 0.024 Report level label = 0.008 Pct Recovery = 84% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl SpecificMix = 041415 Laboratory ID = 20151900132 Lab Value = 0.036 Expected Conc. = 0.024 Report level label = 0.008 Pct Recovery = 148% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl SpecificMix = 041415 Laboratory ID = 20140730138 Lab Value = 0.024 Expected Conc. = 0.0222 Report level label = 0.008 Pct Recovery = 107% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 1473000 Laboratory ID = 20133470008 Lab Value = 0.026 Expected Conc. = 0.0222 Report level label = 0.008 Pct Recovery = 116% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl SpecificMix = 1473000 Laboratory ID = 20133310030 Lab Value = 0.034 Expected Conc. = 0.0222 Report level label = 0.008 Pct Recovery = 151% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl SpecificMix = 1473000 Laboratory ID = 20131790009 Lab Value = 0.032 Expected Conc. = 0.0222 Report level label = 0.008 Pct Recovery = 144% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl SpecificMix = 1473000 Laboratory ID = 20131650073 Lab Value = 0.028 Expected Conc. = 0.0222 Report level label = 0.008 Pct Recovery = 127% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl SpecificMix = 1473000 Laboratory ID = 20133050050 Lab Value = 0.024 Expected Conc. = 0.022 Report level label = 0.008 Pct Recovery = 107% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl SpecificMix = T1130514013 Laboratory ID = 20132280016 Lab Value = 0.024 Expected Conc. = 0.022 Report level label = 0.008 Pct Recovery = 109% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl SpecificMix = T1130514013 Laboratory ID = 20172020035 Lab Value = 0.031 Expected Conc. = 0.0212 Report level label = 0.008 Pct Recovery = 146% Analysis Date = 11/07/17 SpikeMix = Abs 071717Pest: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 071717Pest Laboratory ID = 20171510080 Lab Value = 0.023 Expected Conc. = 0.0201 Report level label = 0.008 Pct Recovery = 115% Analysis Date = 06/09/17 SpikeMix = Supelco LC20138V: 40 µl & Crescent 03FF076: 40 µl SpecificMix = LC20138V Laboratory ID = 20162520001 Lab Value = 0.029 Expected Conc. = 0.0201 Report level label = 0.008 Pct Recovery = 142% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl SpecificMix = LC20138V Laboratory ID = 20162660005 Lab Value = 0.021 Expected Conc. = 0.0201 Report level label = 0.008 Pct Recovery = 103% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl SpecificMix = LC20138V Laboratory ID = 20162020124 Lab Value = 0.022 Expected Conc. = 0.0201 Report level label = 0.008 Pct Recovery = 108% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl SpecificMix = LC20138V Laboratory ID = 20171940002 Lab Value = 0.026 Expected Conc. = 0.02 Report level label = 0.008 Pct Recovery = 131% Analysis Date = 11/10/17 SpikeMix = ChemService 5054800: 40 µl & NSI 041816: 40 µl SpecificMix = 5054800 Laboratory ID = 20170460061 Lab Value = 0.022 Expected Conc. = 0.02 Report level label = 0.008 Pct Recovery = 110% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl SpecificMix = 5054800 Laboratory ID = 20163560019 Lab Value = 0.023 Expected Conc. = 0.02 Report level label = 0.008 Pct Recovery = 116% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl SpecificMix = 5054800 Laboratory ID = 20162150213 Lab Value = 0.027 Expected Conc. = 0.02 Report level label = 0.008 Pct Recovery = 135% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl SpecificMix = 5054800 Laboratory ID = 20140860102 Lab Value = 0.020 Expected Conc. = 0.02 Report level label = 0.008 Pct Recovery = 98% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl SpecificMix = A093651 Laboratory ID = 20133400002 Lab Value = 0.020 Expected Conc. = 0.02 Report level label = 0.008 Pct Recovery = 100% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = A093651 Laboratory ID = 20132910008 Lab Value = 0.021 Expected Conc. = 0.02 Report level label = 0.008 Pct Recovery = 107% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = A093651 Laboratory ID = 20131920149 Lab Value = 0.021 Expected Conc. = 0.02 Report level label = 0.008 Pct Recovery = 103% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl SpecificMix = A093651 Laboratory ID = 20131230084 Lab Value = 0.027 Expected Conc. = 0.02 Report level label = 0.008 Pct Recovery = 135% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl SpecificMix = A088380 Laboratory ID = 20130650005 Lab Value = 0.018 Expected Conc. = 0.02 Report level label = 0.008 Pct Recovery = 92% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl SpecificMix = A088380 Laboratory ID = 20130390105 Lab Value = 0.018 Expected Conc. = 0.02 Report level label = 0.008 Pct Recovery = 92% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl SpecificMix = T1120530013 Laboratory ID = 20150150115 Lab Value = 0.021 Expected Conc. = 0.016 Report level label = 0.008 Pct Recovery = 130% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl SpecificMix = LC06435 Laboratory ID = 20141910243 Lab Value = 0.015 Expected Conc. = 0.016 Report level label = 0.008 Pct Recovery = 91% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = LC06435 Laboratory ID = 20141840097 Lab Value = 0.017 Expected Conc. = 0.016 Report level label = 0.008 Pct Recovery = 103% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl SpecificMix = LC06435 Laboratory ID = 20173120093 Lab Value = 0.021 Expected Conc. = 0.0159 Report level label = 0.008 Pct Recovery = 131% Analysis Date = 03/10/18 SpikeMix = ChemService 6472100: 30 µl & ChemService 6537100: 30 µl SpecificMix = 6537100 Laboratory ID = 20172780018 Lab Value = 0.020 Expected Conc. = 0.0159 Report level label = 0.008 Pct Recovery = 126% Analysis Date = 02/08/18 SpikeMix = ChemService 6537100: 30 µl & Abs 071817Pest: 30 µl SpecificMix = 6537100 Laboratory ID = 20141640076 Lab Value = 0.018 Expected Conc. = 0.0159 Report level label = 0.008 Pct Recovery = 116% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = 03DD006 Laboratory ID = 20141420140 Lab Value = 0.016 Expected Conc. = 0.0159 Report level label = 0.008 Pct Recovery = 102% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 03DD006 Laboratory ID = 20141080004 Lab Value = 0.018 Expected Conc. = 0.0159 Report level label = 0.008 Pct Recovery = 114% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl SpecificMix = 03DD006 Laboratory ID = 20161050143 Lab Value = 0.014 Expected Conc. = 0.012 Report level label = 0.008 Pct Recovery = 116% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 041415 Laboratory ID = 20160560044 Lab Value = 0.013 Expected Conc. = 0.012 Report level label = 0.008 Pct Recovery = 112% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl SpecificMix = 041415 Laboratory ID = 20160210080 Lab Value = 0.011 Expected Conc. = 0.012 Report level label = 0.008 Pct Recovery = 93% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 041415 Laboratory ID = 20160070059 Lab Value = 0.011 Expected Conc. = 0.012 Report level label = 0.008 Pct Recovery = 93% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = EN150514012 Laboratory ID = 20153160001 Lab Value = 0.013 Expected Conc. = 0.012 Report level label = 0.008 Pct Recovery = 106% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = EN150514012 Laboratory ID = 20152950078 Lab Value = 0.009 Expected Conc. = 0.012 Report level label = 0.008 Pct Recovery = 77% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 041415 Laboratory ID = 20152040177 Lab Value = 0.021 Expected Conc. = 0.012 Report level label = 0.008 Pct Recovery = 176% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl SpecificMix = 041415 Laboratory ID = 20151760208 Lab Value = 0.019 Expected Conc. = 0.012 Report level label = 0.008 Pct Recovery = 158% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl SpecificMix = EN150514012 Laboratory ID = 20151480170 Lab Value = 0.014 Expected Conc. = 0.012 Report level label = 0.008 Pct Recovery = 118% Analysis Date = 06/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150514012 Laboratory ID = 20151210037 Lab Value = 0.013 Expected Conc. = 0.012 Report level label = 0.008 Pct Recovery = 109% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 041415 Analysis Date = 03/10/18 Pct Recovery = 123% Analysis Date = 02/28/18 Pct Recovery = 123% Analysis Date = 02/28/18 Pct Recovery = 123% Analysis Date = 02/19/18 Pct Recovery = 122% Analysis Date = 02/19/18 Pct Recovery = 122% Analysis Date = 02/09/18 Pct Recovery = 122% Analysis Date = 02/09/18 Pct Recovery = 122% Analysis Date = 01/31/18 Pct Recovery = 122% Analysis Date = 01/31/18 Pct Recovery = 122% Analysis Date = 01/22/18 Pct Recovery = 122% Analysis Date = 01/22/18 Pct Recovery = 122% Analysis Date = 01/12/18 Pct Recovery = 122% Analysis Date = 01/12/18 Pct Recovery = 122% Analysis Date = 01/03/18 Pct Recovery = 121% Analysis Date = 01/03/18 Pct Recovery = 121% Analysis Date = 12/24/17 Pct Recovery = 121% Analysis Date = 12/24/17 Pct Recovery = 121% Analysis Date = 12/15/17 Pct Recovery = 121% Analysis Date = 12/15/17 Pct Recovery = 121% Analysis Date = 12/06/17 Pct Recovery = 121% Analysis Date = 12/06/17 Pct Recovery = 121% Analysis Date = 11/26/17 Pct Recovery = 120% Analysis Date = 11/26/17 Pct Recovery = 120% Analysis Date = 11/17/17 Pct Recovery = 120% Analysis Date = 11/17/17 Pct Recovery = 120% Analysis Date = 11/07/17 Pct Recovery = 120% Analysis Date = 11/07/17 Pct Recovery = 120% Analysis Date = 10/29/17 Pct Recovery = 120% Analysis Date = 10/29/17 Pct Recovery = 120% Analysis Date = 10/20/17 Pct Recovery = 120% Analysis Date = 10/20/17 Pct Recovery = 120% Analysis Date = 10/10/17 Pct Recovery = 119% Analysis Date = 10/10/17 Pct Recovery = 119% Analysis Date = 10/01/17 Pct Recovery = 119% Analysis Date = 10/01/17 Pct Recovery = 119% Analysis Date = 09/21/17 Pct Recovery = 119% Analysis Date = 09/21/17 Pct Recovery = 119% Analysis Date = 09/12/17 Pct Recovery = 119% Analysis Date = 09/12/17 Pct Recovery = 119% Analysis Date = 09/03/17 Pct Recovery = 118% Analysis Date = 09/03/17 Pct Recovery = 118% Analysis Date = 08/24/17 Pct Recovery = 118% Analysis Date = 08/24/17 Pct Recovery = 118% Analysis Date = 08/15/17 Pct Recovery = 118% Analysis Date = 08/15/17 Pct Recovery = 118% Analysis Date = 08/05/17 Pct Recovery = 118% Analysis Date = 08/05/17 Pct Recovery = 118% Analysis Date = 07/27/17 Pct Recovery = 118% Analysis Date = 07/27/17 Pct Recovery = 118% Analysis Date = 07/18/17 Pct Recovery = 117% Analysis Date = 07/18/17 Pct Recovery = 117% Analysis Date = 07/08/17 Pct Recovery = 117% Analysis Date = 07/08/17 Pct Recovery = 117% Analysis Date = 06/29/17 Pct Recovery = 117% Analysis Date = 06/29/17 Pct Recovery = 117% Analysis Date = 06/19/17 Pct Recovery = 117% Analysis Date = 06/19/17 Pct Recovery = 117% Analysis Date = 06/10/17 Pct Recovery = 117% Analysis Date = 06/10/17 Pct Recovery = 117% Analysis Date = 06/01/17 Pct Recovery = 116% Analysis Date = 06/01/17 Pct Recovery = 116% Analysis Date = 05/22/17 Pct Recovery = 116% Analysis Date = 05/22/17 Pct Recovery = 116% Analysis Date = 05/13/17 Pct Recovery = 116% Analysis Date = 05/13/17 Pct Recovery = 116% Analysis Date = 05/03/17 Pct Recovery = 116% Analysis Date = 05/03/17 Pct Recovery = 116% Analysis Date = 04/24/17 Pct Recovery = 116% Analysis Date = 04/24/17 Pct Recovery = 116% Analysis Date = 04/15/17 Pct Recovery = 115% Analysis Date = 04/15/17 Pct Recovery = 115% Analysis Date = 04/05/17 Pct Recovery = 115% Analysis Date = 04/05/17 Pct Recovery = 115% Analysis Date = 03/27/17 Pct Recovery = 115% Analysis Date = 03/27/17 Pct Recovery = 115% Analysis Date = 03/17/17 Pct Recovery = 115% Analysis Date = 03/17/17 Pct Recovery = 115% Analysis Date = 03/08/17 Pct Recovery = 115% Analysis Date = 03/08/17 Pct Recovery = 115% Analysis Date = 02/27/17 Pct Recovery = 115% Analysis Date = 02/27/17 Pct Recovery = 115% Analysis Date = 02/17/17 Pct Recovery = 114% Analysis Date = 02/17/17 Pct Recovery = 114% Analysis Date = 02/08/17 Pct Recovery = 114% Analysis Date = 02/08/17 Pct Recovery = 114% Analysis Date = 01/29/17 Pct Recovery = 114% Analysis Date = 01/29/17 Pct Recovery = 114% Analysis Date = 01/20/17 Pct Recovery = 114% Analysis Date = 01/20/17 Pct Recovery = 114% Analysis Date = 01/11/17 Pct Recovery = 114% Analysis Date = 01/11/17 Pct Recovery = 114% Analysis Date = 01/01/17 Pct Recovery = 114% Analysis Date = 01/01/17 Pct Recovery = 114% Analysis Date = 12/23/16 Pct Recovery = 113% Analysis Date = 12/23/16 Pct Recovery = 113% Analysis Date = 12/13/16 Pct Recovery = 113% Analysis Date = 12/13/16 Pct Recovery = 113% Analysis Date = 12/04/16 Pct Recovery = 113% Analysis Date = 12/04/16 Pct Recovery = 113% Analysis Date = 11/25/16 Pct Recovery = 113% Analysis Date = 11/25/16 Pct Recovery = 113% Analysis Date = 11/15/16 Pct Recovery = 113% Analysis Date = 11/15/16 Pct Recovery = 113% Analysis Date = 11/06/16 Pct Recovery = 113% Analysis Date = 11/06/16 Pct Recovery = 113% Analysis Date = 10/27/16 Pct Recovery = 112% Analysis Date = 10/27/16 Pct Recovery = 112% Analysis Date = 10/18/16 Pct Recovery = 112% Analysis Date = 10/18/16 Pct Recovery = 112% Analysis Date = 10/09/16 Pct Recovery = 112% Analysis Date = 10/09/16 Pct Recovery = 112% Analysis Date = 09/29/16 Pct Recovery = 112% Analysis Date = 09/29/16 Pct Recovery = 112% Analysis Date = 09/20/16 Pct Recovery = 112% Analysis Date = 09/20/16 Pct Recovery = 112% Analysis Date = 09/10/16 Pct Recovery = 112% Analysis Date = 09/10/16 Pct Recovery = 112% Analysis Date = 09/01/16 Pct Recovery = 112% Analysis Date = 09/01/16 Pct Recovery = 112% Analysis Date = 08/23/16 Pct Recovery = 112% Analysis Date = 08/23/16 Pct Recovery = 112% Analysis Date = 08/13/16 Pct Recovery = 112% Analysis Date = 08/13/16 Pct Recovery = 112% Analysis Date = 08/04/16 Pct Recovery = 112% Analysis Date = 08/04/16 Pct Recovery = 112% Analysis Date = 07/25/16 Pct Recovery = 112% Analysis Date = 07/25/16 Pct Recovery = 112% Analysis Date = 07/16/16 Pct Recovery = 112% Analysis Date = 07/16/16 Pct Recovery = 112% Analysis Date = 07/07/16 Pct Recovery = 112% Analysis Date = 07/07/16 Pct Recovery = 112% Analysis Date = 06/27/16 Pct Recovery = 112% Analysis Date = 06/27/16 Pct Recovery = 112% Analysis Date = 06/18/16 Pct Recovery = 112% Analysis Date = 06/18/16 Pct Recovery = 112% Analysis Date = 06/08/16 Pct Recovery = 112% Analysis Date = 06/08/16 Pct Recovery = 112% Analysis Date = 05/30/16 Pct Recovery = 112% Analysis Date = 05/30/16 Pct Recovery = 112% Analysis Date = 05/21/16 Pct Recovery = 112% Analysis Date = 05/21/16 Pct Recovery = 112% Analysis Date = 05/11/16 Pct Recovery = 112% Analysis Date = 05/11/16 Pct Recovery = 112% Analysis Date = 05/02/16 Pct Recovery = 112% Analysis Date = 05/02/16 Pct Recovery = 112% Analysis Date = 04/22/16 Pct Recovery = 112% Analysis Date = 04/22/16 Pct Recovery = 112% Analysis Date = 04/13/16 Pct Recovery = 112% Analysis Date = 04/13/16 Pct Recovery = 112% Analysis Date = 04/04/16 Pct Recovery = 113% Analysis Date = 04/04/16 Pct Recovery = 113% Analysis Date = 03/25/16 Pct Recovery = 113% Analysis Date = 03/25/16 Pct Recovery = 113% Analysis Date = 03/16/16 Pct Recovery = 114% Analysis Date = 03/16/16 Pct Recovery = 114% Analysis Date = 03/06/16 Pct Recovery = 114% Analysis Date = 03/06/16 Pct Recovery = 114% Analysis Date = 02/26/16 Pct Recovery = 115% Analysis Date = 02/26/16 Pct Recovery = 115% Analysis Date = 02/17/16 Pct Recovery = 115% Analysis Date = 02/17/16 Pct Recovery = 115% Analysis Date = 02/07/16 Pct Recovery = 116% Analysis Date = 02/07/16 Pct Recovery = 116% Analysis Date = 01/29/16 Pct Recovery = 116% Analysis Date = 01/29/16 Pct Recovery = 116% Analysis Date = 01/19/16 Pct Recovery = 117% Analysis Date = 01/19/16 Pct Recovery = 117% Analysis Date = 01/10/16 Pct Recovery = 117% Analysis Date = 01/10/16 Pct Recovery = 117% Analysis Date = 01/01/16 Pct Recovery = 118% Analysis Date = 01/01/16 Pct Recovery = 118% Analysis Date = 12/22/15 Pct Recovery = 118% Analysis Date = 12/22/15 Pct Recovery = 118% Analysis Date = 12/13/15 Pct Recovery = 119% Analysis Date = 12/13/15 Pct Recovery = 119% Analysis Date = 12/03/15 Pct Recovery = 119% Analysis Date = 12/03/15 Pct Recovery = 119% Analysis Date = 11/24/15 Pct Recovery = 120% Analysis Date = 11/24/15 Pct Recovery = 120% Analysis Date = 11/15/15 Pct Recovery = 120% Analysis Date = 11/15/15 Pct Recovery = 120% Analysis Date = 11/05/15 Pct Recovery = 121% Analysis Date = 11/05/15 Pct Recovery = 121% Analysis Date = 10/27/15 Pct Recovery = 121% Analysis Date = 10/27/15 Pct Recovery = 121% Analysis Date = 10/17/15 Pct Recovery = 122% Analysis Date = 10/17/15 Pct Recovery = 122% Analysis Date = 10/08/15 Pct Recovery = 122% Analysis Date = 10/08/15 Pct Recovery = 122% Analysis Date = 09/29/15 Pct Recovery = 123% Analysis Date = 09/29/15 Pct Recovery = 123% Analysis Date = 09/19/15 Pct Recovery = 123% Analysis Date = 09/19/15 Pct Recovery = 123% Analysis Date = 09/10/15 Pct Recovery = 124% Analysis Date = 09/10/15 Pct Recovery = 124% Analysis Date = 08/31/15 Pct Recovery = 124% Analysis Date = 08/31/15 Pct Recovery = 124% Analysis Date = 08/22/15 Pct Recovery = 125% Analysis Date = 08/22/15 Pct Recovery = 125% Analysis Date = 08/13/15 Pct Recovery = 125% Analysis Date = 08/13/15 Pct Recovery = 125% Analysis Date = 08/03/15 Pct Recovery = 126% Analysis Date = 08/03/15 Pct Recovery = 126% Analysis Date = 07/25/15 Pct Recovery = 126% Analysis Date = 07/25/15 Pct Recovery = 126% Analysis Date = 07/15/15 Pct Recovery = 127% Analysis Date = 07/15/15 Pct Recovery = 127% Analysis Date = 07/06/15 Pct Recovery = 127% Analysis Date = 07/06/15 Pct Recovery = 127% Analysis Date = 06/27/15 Pct Recovery = 127% Analysis Date = 06/27/15 Pct Recovery = 127% Analysis Date = 06/17/15 Pct Recovery = 128% Analysis Date = 06/17/15 Pct Recovery = 128% Analysis Date = 06/08/15 Pct Recovery = 128% Analysis Date = 06/08/15 Pct Recovery = 128% Analysis Date = 05/29/15 Pct Recovery = 129% Analysis Date = 05/29/15 Pct Recovery = 129% Analysis Date = 05/20/15 Pct Recovery = 129% Analysis Date = 05/20/15 Pct Recovery = 129% Analysis Date = 05/11/15 Pct Recovery = 130% Analysis Date = 05/11/15 Pct Recovery = 130% Analysis Date = 05/01/15 Pct Recovery = 130% Analysis Date = 05/01/15 Pct Recovery = 130% Analysis Date = 04/22/15 Pct Recovery = 131% Analysis Date = 04/22/15 Pct Recovery = 131% Analysis Date = 04/12/15 Pct Recovery = 131% Analysis Date = 04/12/15 Pct Recovery = 131% Analysis Date = 04/03/15 Pct Recovery = 132% Analysis Date = 04/03/15 Pct Recovery = 132% Analysis Date = 03/25/15 Pct Recovery = 132% Analysis Date = 03/25/15 Pct Recovery = 132% Analysis Date = 03/15/15 Pct Recovery = 132% Analysis Date = 03/15/15 Pct Recovery = 132% Analysis Date = 03/06/15 Pct Recovery = 132% Analysis Date = 03/06/15 Pct Recovery = 132% Analysis Date = 02/24/15 Pct Recovery = 133% Analysis Date = 02/24/15 Pct Recovery = 133% Analysis Date = 02/15/15 Pct Recovery = 133% Analysis Date = 02/15/15 Pct Recovery = 133% Analysis Date = 02/06/15 Pct Recovery = 133% Analysis Date = 02/06/15 Pct Recovery = 133% Analysis Date = 01/27/15 Pct Recovery = 133% Analysis Date = 01/27/15 Pct Recovery = 133% Analysis Date = 01/18/15 Pct Recovery = 134% Analysis Date = 01/18/15 Pct Recovery = 134% Analysis Date = 01/08/15 Pct Recovery = 134% Analysis Date = 01/08/15 Pct Recovery = 134% Analysis Date = 12/30/14 Pct Recovery = 134% Analysis Date = 12/30/14 Pct Recovery = 134% Analysis Date = 12/21/14 Pct Recovery = 135% Analysis Date = 12/21/14 Pct Recovery = 135% Analysis Date = 12/11/14 Pct Recovery = 135% Analysis Date = 12/11/14 Pct Recovery = 135% Analysis Date = 12/02/14 Pct Recovery = 135% Analysis Date = 12/02/14 Pct Recovery = 135% Analysis Date = 11/22/14 Pct Recovery = 135% Analysis Date = 11/22/14 Pct Recovery = 135% Analysis Date = 11/13/14 Pct Recovery = 136% Analysis Date = 11/13/14 Pct Recovery = 136% Analysis Date = 11/04/14 Pct Recovery = 136% Analysis Date = 11/04/14 Pct Recovery = 136% Analysis Date = 10/25/14 Pct Recovery = 136% Analysis Date = 10/25/14 Pct Recovery = 136% Analysis Date = 10/16/14 Pct Recovery = 136% Analysis Date = 10/16/14 Pct Recovery = 136% Analysis Date = 10/06/14 Pct Recovery = 137% Analysis Date = 10/06/14 Pct Recovery = 137% Analysis Date = 09/27/14 Pct Recovery = 136% Analysis Date = 09/27/14 Pct Recovery = 136% Analysis Date = 09/18/14 Pct Recovery = 136% Analysis Date = 09/18/14 Pct Recovery = 136% Analysis Date = 09/08/14 Pct Recovery = 135% Analysis Date = 09/08/14 Pct Recovery = 135% Analysis Date = 08/30/14 Pct Recovery = 134% Analysis Date = 08/30/14 Pct Recovery = 134% Analysis Date = 08/20/14 Pct Recovery = 134% Analysis Date = 08/20/14 Pct Recovery = 134% Analysis Date = 08/11/14 Pct Recovery = 133% Analysis Date = 08/11/14 Pct Recovery = 133% Analysis Date = 08/02/14 Pct Recovery = 133% Analysis Date = 08/02/14 Pct Recovery = 133% Analysis Date = 07/23/14 Pct Recovery = 132% Analysis Date = 07/23/14 Pct Recovery = 132% Analysis Date = 07/14/14 Pct Recovery = 131% Analysis Date = 07/14/14 Pct Recovery = 131% Analysis Date = 07/04/14 Pct Recovery = 131% Analysis Date = 07/04/14 Pct Recovery = 131% Analysis Date = 06/25/14 Pct Recovery = 130% Analysis Date = 06/25/14 Pct Recovery = 130% Analysis Date = 06/16/14 Pct Recovery = 130% Analysis Date = 06/16/14 Pct Recovery = 130% Analysis Date = 06/06/14 Pct Recovery = 129% Analysis Date = 06/06/14 Pct Recovery = 129% Analysis Date = 05/28/14 Pct Recovery = 129% Analysis Date = 05/28/14 Pct Recovery = 129% Analysis Date = 05/18/14 Pct Recovery = 128% Analysis Date = 05/18/14 Pct Recovery = 128% Analysis Date = 05/09/14 Pct Recovery = 128% Analysis Date = 05/09/14 Pct Recovery = 128% Analysis Date = 04/30/14 Pct Recovery = 127% Analysis Date = 04/30/14 Pct Recovery = 127% Analysis Date = 04/20/14 Pct Recovery = 126% Analysis Date = 04/20/14 Pct Recovery = 126% Analysis Date = 04/11/14 Pct Recovery = 126% Analysis Date = 04/11/14 Pct Recovery = 126% Analysis Date = 04/01/14 Pct Recovery = 125% Analysis Date = 04/01/14 Pct Recovery = 125% Analysis Date = 03/23/14 Pct Recovery = 124% Analysis Date = 03/23/14 Pct Recovery = 124% Analysis Date = 03/14/14 Pct Recovery = 123% Analysis Date = 03/14/14 Pct Recovery = 123% Analysis Date = 03/04/14 Pct Recovery = 122% Analysis Date = 03/04/14 Pct Recovery = 122% Analysis Date = 02/23/14 Pct Recovery = 121% Analysis Date = 02/23/14 Pct Recovery = 121% Analysis Date = 02/13/14 Pct Recovery = 120% Analysis Date = 02/13/14 Pct Recovery = 120% Analysis Date = 02/04/14 Pct Recovery = 120% Analysis Date = 02/04/14 Pct Recovery = 120% Analysis Date = 01/26/14 Pct Recovery = 119% Analysis Date = 01/26/14 Pct Recovery = 119% Analysis Date = 01/16/14 Pct Recovery = 118% Analysis Date = 01/16/14 Pct Recovery = 118% Analysis Date = 01/07/14 Pct Recovery = 117% Analysis Date = 01/07/14 Pct Recovery = 117% Analysis Date = 12/28/13 Pct Recovery = 116% Analysis Date = 12/28/13 Pct Recovery = 116% Analysis Date = 12/19/13 Pct Recovery = 116% Analysis Date = 12/19/13 Pct Recovery = 116% Analysis Date = 12/10/13 Pct Recovery = 115% Analysis Date = 12/10/13 Pct Recovery = 115% Analysis Date = 11/30/13 Pct Recovery = 114% Analysis Date = 11/30/13 Pct Recovery = 114% Analysis Date = 11/21/13 Pct Recovery = 113% Analysis Date = 11/21/13 Pct Recovery = 113% Analysis Date = 11/11/13 Pct Recovery = 112% Analysis Date = 11/11/13 Pct Recovery = 112% Analysis Date = 11/02/13 Pct Recovery = 111% Analysis Date = 11/02/13 Pct Recovery = 111% Analysis Date = 10/24/13 Pct Recovery = 111% Analysis Date = 10/24/13 Pct Recovery = 111% Analysis Date = 10/14/13 Pct Recovery = 110% Analysis Date = 10/14/13 Pct Recovery = 110% Analysis Date = 10/05/13 Pct Recovery = 109% Analysis Date = 10/05/13 Pct Recovery = 109% Analysis Date = 09/25/13 Pct Recovery = 108% Analysis Date = 09/25/13 Pct Recovery = 108% Analysis Date = 09/16/13 Pct Recovery = 108% Analysis Date = 09/16/13 Pct Recovery = 108% Analysis Date = 09/07/13 Pct Recovery = 107% Analysis Date = 09/07/13 Pct Recovery = 107% Analysis Date = 08/28/13 Pct Recovery = 106% Analysis Date = 08/28/13 Pct Recovery = 106% Analysis Date = 08/19/13 Pct Recovery = 105% Analysis Date = 08/19/13 Pct Recovery = 105% Analysis Date = 08/09/13 Pct Recovery = 104% Analysis Date = 08/09/13 Pct Recovery = 104% Analysis Date = 07/31/13 Pct Recovery = 104% Analysis Date = 07/31/13 Pct Recovery = 104% Analysis Date = 07/22/13 Pct Recovery = 103% Analysis Date = 07/22/13 Pct Recovery = 103% Analysis Date = 07/12/13 Pct Recovery = 102% Analysis Date = 07/12/13 Pct Recovery = 102% Analysis Date = 07/03/13 Pct Recovery = 102% Analysis Date = 07/03/13 Pct Recovery = 102% Analysis Date = 06/23/13 Pct Recovery = 101% Analysis Date = 06/23/13 Pct Recovery = 101% Analysis Date = 06/14/13 Pct Recovery = 100% Analysis Date = 06/14/13 Pct Recovery = 100% Analysis Date = 06/05/13 Pct Recovery = 99% Analysis Date = 06/05/13 Pct Recovery = 99% Analysis Date = 05/26/13 Pct Recovery = 99% Analysis Date = 05/26/13 Pct Recovery = 99% Analysis Date = 05/17/13 Pct Recovery = 98% Analysis Date = 05/17/13 Pct Recovery = 98% Analysis Date = 05/07/13 Pct Recovery = 97% Analysis Date = 05/07/13 Pct Recovery = 97% Analysis Date = 04/28/13 Pct Recovery = 97% Analysis Date = 04/28/13 Pct Recovery = 97% Analysis Date = 04/19/13 Pct Recovery = 96% Analysis Date = 04/19/13 Pct Recovery = 96% Analysis Date = 04/09/13 Pct Recovery = 95% Analysis Date = 04/09/13 Pct Recovery = 95% Analysis Date = 03/31/13 Pct Recovery = 95% Analysis Date = 03/31/13 Pct Recovery = 95% Analysis Date = 03/21/13 Pct Recovery = 94% Analysis Date = 03/21/13 Pct Recovery = 94% Analysis Date = 03/12/13 Pct Recovery = 93% Analysis Date = 03/12/13 Pct Recovery = 93% Analysis Date = 03/03/13 Pct Recovery = 93% Analysis Date = 03/03/13 Pct Recovery = 93% Analysis Date = 02/21/13 Pct Recovery = 92% Analysis Date = 02/21/13 Pct Recovery = 92% Analysis Date = 02/12/13 Pct Recovery = 92% Analysis Date = 02/12/13 Pct Recovery = 92% Analysis Date = 02/02/13 Pct Recovery = 91% Analysis Date = 02/02/13 Pct Recovery = 91% Analysis Date = 01/24/13 Pct Recovery = 90% Analysis Date = 01/24/13 Pct Recovery = 90% Analysis Date = 01/15/13 Pct Recovery = 90% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
PARATHION-METHYL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 79 118% 42% 108% 23%
Total 79 118% 42% 108% 23%

Sample Statistics
PARATHION-METHYL

Characteristic N % % Basis
Plotted 79 99% Spiked
Estimated Values 3 4% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 80 .  
False Negatives 1 1% 1 out of 80
Not Spiked 34 .  
False Positives 0 0% 0 out of 34

OBSP Determination:
PENDIMETHALIN
METHOD: 2033 , TESTIDCODE: 82683GCM35

Laboratory ID = 20132490342 Lab Value = 0.098 Expected Conc. = 0.125 Report level label = 0.012 Pct Recovery = 78% Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20172510330 Lab Value = 0.061 Expected Conc. = 0.08 Report level label = 0.012 Pct Recovery = 76% Analysis Date = 12/29/17 SpikeMix = ChemService 6537100: 100 µl & Abs 071817Pest: 100 µl SpecificMix = 071817Pest Laboratory ID = 20162860079 Lab Value = 0.059 Expected Conc. = 0.075 Report level label = 0.012 Pct Recovery = 79% Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl SpecificMix = 060916 Laboratory ID = 20163150006 Lab Value = 0.060 Expected Conc. = 0.075 Report level label = 0.012 Pct Recovery = 80% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl SpecificMix = 060916 Laboratory ID = 20152610011 Lab Value = 0.059 Expected Conc. = 0.0725 Report level label = 0.012 Pct Recovery = 81% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl SpecificMix = 0406-15-01 Laboratory ID = 20152460215 Lab Value = 0.047 Expected Conc. = 0.0725 Report level label = 0.012 Pct Recovery = 65% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl SpecificMix = 0406-15-01 Laboratory ID = 20132140002 Lab Value = 0.050 Expected Conc. = 0.0626 Report level label = 0.012 Pct Recovery = 80% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl SpecificMix = LB99392 Laboratory ID = 20131370001 Lab Value = 0.061 Expected Conc. = 0.0626 Report level label = 0.012 Pct Recovery = 98% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl SpecificMix = LB99392 Laboratory ID = 20140370077 Lab Value = 0.050 Expected Conc. = 0.0625 Report level label = 0.012 Pct Recovery = 80% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20132560001 Lab Value = 0.055 Expected Conc. = 0.0625 Report level label = 0.012 Pct Recovery = 88% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20171660002 Lab Value = 0.049 Expected Conc. = 0.06 Report level label = 0.012 Pct Recovery = 82% Analysis Date = 08/23/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = 060916 Laboratory ID = 20170190026 Lab Value = 0.052 Expected Conc. = 0.06 Report level label = 0.012 Pct Recovery = 87% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = 060916 Laboratory ID = 20171380001 Lab Value = 0.047 Expected Conc. = 0.052 Report level label = 0.012 Pct Recovery = 91% Analysis Date = 06/07/17 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 041816 Laboratory ID = 20170740063 Lab Value = 0.051 Expected Conc. = 0.052 Report level label = 0.012 Pct Recovery = 98% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl SpecificMix = 041816 Laboratory ID = 20161740258 Lab Value = 0.041 Expected Conc. = 0.052 Report level label = 0.012 Pct Recovery = 79% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 041816 Laboratory ID = 20130940097 Lab Value = 0.036 Expected Conc. = 0.05 Report level label = 0.012 Pct Recovery = 73% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = 0507-12-04.2 Laboratory ID = 20130810108 Lab Value = 0.035 Expected Conc. = 0.05 Report level label = 0.012 Pct Recovery = 70% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl SpecificMix = LB92783 Laboratory ID = 20130100066 Lab Value = 0.046 Expected Conc. = 0.05 Report level label = 0.012 Pct Recovery = 91% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl SpecificMix = LB92783 Laboratory ID = 20123560092 Lab Value = 0.043 Expected Conc. = 0.05 Report level label = 0.012 Pct Recovery = 87% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = 0507-12-04.2 Laboratory ID = 20143240095 Lab Value = 0.045 Expected Conc. = 0.048 Report level label = 0.012 Pct Recovery = 94% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl SpecificMix = 032714 Laboratory ID = 20142270001 Lab Value = 0.035 Expected Conc. = 0.048 Report level label = 0.012 Pct Recovery = 73% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl SpecificMix = 032714 Laboratory ID = 20141220025 Lab Value = 0.042 Expected Conc. = 0.048 Report level label = 0.012 Pct Recovery = 88% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl SpecificMix = 032714 Laboratory ID = 20150430092 Lab Value = 0.043 Expected Conc. = 0.0479 Report level label = 0.012 Pct Recovery = 90% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl SpecificMix = E1140407002 Laboratory ID = 20143110108 Lab Value = 0.043 Expected Conc. = 0.0479 Report level label = 0.012 Pct Recovery = 89% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl SpecificMix = E1140407002 Laboratory ID = 20142720002 Lab Value = 0.040 Expected Conc. = 0.0479 Report level label = 0.012 Pct Recovery = 84% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl SpecificMix = E1140407002 Laboratory ID = 20141770149 Lab Value = 0.039 Expected Conc. = 0.0479 Report level label = 0.012 Pct Recovery = 81% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl SpecificMix = E1140407002 Laboratory ID = 20181430122 Lab Value = 0.048 Expected Conc. = 0.04 Report level label = 0.012 Pct Recovery = 120% Analysis Date = 06/20/18 SpikeMix = Abs 071817Pest: 50 µl & Spex Organics EN170808006: 50 µl SpecificMix = 071817Pest Laboratory ID = 20173480003 Lab Value = 0.038 Expected Conc. = 0.04 Report level label = 0.012 Pct Recovery = 96% Analysis Date = 04/05/18 SpikeMix = Abs 071717Pest: 50 µl & ChemService 6567600: 50 µl SpecificMix = 6567600 Laboratory ID = 20172560101 Lab Value = 0.043 Expected Conc. = 0.04 Report level label = 0.012 Pct Recovery = 108% Analysis Date = 12/22/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6567600: 50 µl SpecificMix = 6567600 Laboratory ID = 20160770090 Lab Value = 0.033 Expected Conc. = 0.0362 Report level label = 0.012 Pct Recovery = 90% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20160630046 Lab Value = 0.037 Expected Conc. = 0.0362 Report level label = 0.012 Pct Recovery = 102% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20153510109 Lab Value = 0.029 Expected Conc. = 0.0362 Report level label = 0.012 Pct Recovery = 79% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20153440001 Lab Value = 0.031 Expected Conc. = 0.0362 Report level label = 0.012 Pct Recovery = 84% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20161260151 Lab Value = 0.034 Expected Conc. = 0.036 Report level label = 0.012 Pct Recovery = 96% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = 3851600 Laboratory ID = 20151550293 Lab Value = 0.027 Expected Conc. = 0.036 Report level label = 0.012 Pct Recovery = 76% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl SpecificMix = 3851600 Laboratory ID = 20151270112 Lab Value = 0.029 Expected Conc. = 0.036 Report level label = 0.012 Pct Recovery = 82% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl SpecificMix = 3851600 Laboratory ID = 20171160110 Lab Value = 0.030 Expected Conc. = 0.03 Report level label = 0.012 Pct Recovery = 99% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = 060916 Laboratory ID = 20162520001 Lab Value = 0.030 Expected Conc. = 0.03 Report level label = 0.012 Pct Recovery = 99% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl SpecificMix = 060916 Laboratory ID = 20163560019 Lab Value = 0.036 Expected Conc. = 0.03 Report level label = 0.012 Pct Recovery = 120% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl SpecificMix = 060916 Laboratory ID = 20162380004 Lab Value = 0.026 Expected Conc. = 0.03 Report level label = 0.012 Pct Recovery = 86% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = 060916 Laboratory ID = 20171940002 Lab Value = 0.031 Expected Conc. = 0.026 Report level label = 0.012 Pct Recovery = 118% Analysis Date = 11/10/17 SpikeMix = ChemService 5054800: 40 µl & NSI 041816: 40 µl SpecificMix = 041816 Laboratory ID = 20162020124 Lab Value = 0.024 Expected Conc. = 0.026 Report level label = 0.012 Pct Recovery = 92% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl SpecificMix = 041816 Laboratory ID = 20161600087 Lab Value = 0.022 Expected Conc. = 0.026 Report level label = 0.012 Pct Recovery = 85% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 041816 Laboratory ID = 20161340228 Lab Value = 0.026 Expected Conc. = 0.026 Report level label = 0.012 Pct Recovery = 98% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl SpecificMix = 041816 Laboratory ID = 20161190075 Lab Value = 0.026 Expected Conc. = 0.026 Report level label = 0.012 Pct Recovery = 101% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 041816 Laboratory ID = 20140510043 Lab Value = 0.033 Expected Conc. = 0.025 Report level label = 0.012 Pct Recovery = 133% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl SpecificMix = LB99392 Laboratory ID = 20133470008 Lab Value = 0.021 Expected Conc. = 0.025 Report level label = 0.012 Pct Recovery = 83% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl SpecificMix = LB99392 Laboratory ID = 20133190012 Lab Value = 0.022 Expected Conc. = 0.025 Report level label = 0.012 Pct Recovery = 88% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = LB99392 Laboratory ID = 20133050050 Lab Value = 0.023 Expected Conc. = 0.025 Report level label = 0.012 Pct Recovery = 91% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl SpecificMix = LB99392 Laboratory ID = 20133580036 Lab Value = 0.022 Expected Conc. = 0.025 Report level label = 0.012 Pct Recovery = 86% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20131790009 Lab Value = 0.019 Expected Conc. = 0.025 Report level label = 0.012 Pct Recovery = 76% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20131510026 Lab Value = 0.032 Expected Conc. = 0.025 Report level label = 0.012 Pct Recovery = 126% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20180730064 Lab Value = 0.026 Expected Conc. = 0.024 Report level label = 0.012 Pct Recovery = 110% Analysis Date = 05/16/18 SpikeMix = Abs 071717Pest: 30 µl & Abs 071817Pest: 30 µl SpecificMix = 071817Pest Laboratory ID = 20180050004 Lab Value = 0.023 Expected Conc. = 0.024 Report level label = 0.012 Pct Recovery = 95% Analysis Date = 04/05/18 SpikeMix = Abs 071817Pest: 30 µl & ChemService 6472100: 30 µl SpecificMix = 071817Pest Laboratory ID = 20172780018 Lab Value = 0.032 Expected Conc. = 0.024 Report level label = 0.012 Pct Recovery = 134% Analysis Date = 02/08/18 SpikeMix = ChemService 6537100: 30 µl & Abs 071817Pest: 30 µl SpecificMix = 071817Pest Laboratory ID = 20150150115 Lab Value = 0.027 Expected Conc. = 0.024 Report level label = 0.012 Pct Recovery = 114% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl SpecificMix = 032714 Laboratory ID = 20142820151 Lab Value = 0.022 Expected Conc. = 0.024 Report level label = 0.012 Pct Recovery = 90% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl SpecificMix = 032714 Laboratory ID = 20141490205 Lab Value = 0.017 Expected Conc. = 0.024 Report level label = 0.012 Pct Recovery = 69% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = 032714 Laboratory ID = 20141080004 Lab Value = 0.021 Expected Conc. = 0.024 Report level label = 0.012 Pct Recovery = 88% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl SpecificMix = 032714 Laboratory ID = 20142470041 Lab Value = 0.019 Expected Conc. = 0.024 Report level label = 0.012 Pct Recovery = 81% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141910243 Lab Value = 0.020 Expected Conc. = 0.024 Report level label = 0.012 Pct Recovery = 84% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141640076 Lab Value = 0.018 Expected Conc. = 0.024 Report level label = 0.012 Pct Recovery = 76% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141360094 Lab Value = 0.020 Expected Conc. = 0.024 Report level label = 0.012 Pct Recovery = 81% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = E1140407002 Laboratory ID = 20130510051 Lab Value = 0.022 Expected Conc. = 0.02 Report level label = 0.012 Pct Recovery = 109% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl SpecificMix = 0507-12-04.2 Laboratory ID = 20130390105 Lab Value = 0.015 Expected Conc. = 0.02 Report level label = 0.012 Pct Recovery = 74% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl SpecificMix = LB92783 Laboratory ID = 20152190003 Lab Value = 0.017 Expected Conc. = 0.0181 Report level label = 0.012 Pct Recovery = 92% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = 0406-15-01 Laboratory ID = 20152040177 Lab Value = 0.027 Expected Conc. = 0.0181 Report level label = 0.012 Pct Recovery = 147% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl SpecificMix = 0406-15-01 Laboratory ID = 20160430111 Lab Value = 0.016 Expected Conc. = 0.018 Report level label = 0.012 Pct Recovery = 90% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 3851600 Laboratory ID = 20160210080 Lab Value = 0.016 Expected Conc. = 0.018 Report level label = 0.012 Pct Recovery = 86% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 3851600 Laboratory ID = 20152950078 Lab Value = 0.014 Expected Conc. = 0.018 Report level label = 0.012 Pct Recovery = 76% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 3851600 Laboratory ID = 20153030068 Lab Value = 0.018 Expected Conc. = 0.018 Report level label = 0.012 Pct Recovery = 98% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = 3851600 Laboratory ID = 20151760208 Lab Value = 0.022 Expected Conc. = 0.018 Report level label = 0.012 Pct Recovery = 123% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl SpecificMix = 3851600 Laboratory ID = 20151380009 Lab Value = 0.019 Expected Conc. = 0.018 Report level label = 0.012 Pct Recovery = 103% Analysis Date = 05/30/15 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 3851600 Analysis Date = 06/19/18 Pct Recovery = 106% Analysis Date = 06/10/18 Pct Recovery = 106% Analysis Date = 06/10/18 Pct Recovery = 106% Analysis Date = 05/31/18 Pct Recovery = 106% Analysis Date = 05/31/18 Pct Recovery = 106% Analysis Date = 05/21/18 Pct Recovery = 106% Analysis Date = 05/21/18 Pct Recovery = 106% Analysis Date = 05/11/18 Pct Recovery = 105% Analysis Date = 05/11/18 Pct Recovery = 105% Analysis Date = 05/01/18 Pct Recovery = 105% Analysis Date = 05/01/18 Pct Recovery = 105% Analysis Date = 04/21/18 Pct Recovery = 105% Analysis Date = 04/21/18 Pct Recovery = 105% Analysis Date = 04/11/18 Pct Recovery = 105% Analysis Date = 04/11/18 Pct Recovery = 105% Analysis Date = 04/01/18 Pct Recovery = 104% Analysis Date = 04/01/18 Pct Recovery = 104% Analysis Date = 03/22/18 Pct Recovery = 104% Analysis Date = 03/22/18 Pct Recovery = 104% Analysis Date = 03/12/18 Pct Recovery = 104% Analysis Date = 03/12/18 Pct Recovery = 104% Analysis Date = 03/02/18 Pct Recovery = 104% Analysis Date = 03/02/18 Pct Recovery = 104% Analysis Date = 02/21/18 Pct Recovery = 103% Analysis Date = 02/21/18 Pct Recovery = 103% Analysis Date = 02/11/18 Pct Recovery = 103% Analysis Date = 02/11/18 Pct Recovery = 103% Analysis Date = 02/01/18 Pct Recovery = 103% Analysis Date = 02/01/18 Pct Recovery = 103% Analysis Date = 01/22/18 Pct Recovery = 103% Analysis Date = 01/22/18 Pct Recovery = 103% Analysis Date = 01/12/18 Pct Recovery = 103% Analysis Date = 01/12/18 Pct Recovery = 103% Analysis Date = 01/02/18 Pct Recovery = 102% Analysis Date = 01/02/18 Pct Recovery = 102% Analysis Date = 12/23/17 Pct Recovery = 102% Analysis Date = 12/23/17 Pct Recovery = 102% Analysis Date = 12/13/17 Pct Recovery = 102% Analysis Date = 12/13/17 Pct Recovery = 102% Analysis Date = 12/03/17 Pct Recovery = 102% Analysis Date = 12/03/17 Pct Recovery = 102% Analysis Date = 11/23/17 Pct Recovery = 101% Analysis Date = 11/23/17 Pct Recovery = 101% Analysis Date = 11/13/17 Pct Recovery = 101% Analysis Date = 11/13/17 Pct Recovery = 101% Analysis Date = 11/04/17 Pct Recovery = 101% Analysis Date = 11/04/17 Pct Recovery = 101% Analysis Date = 10/25/17 Pct Recovery = 101% Analysis Date = 10/25/17 Pct Recovery = 101% Analysis Date = 10/15/17 Pct Recovery = 101% Analysis Date = 10/15/17 Pct Recovery = 101% Analysis Date = 10/05/17 Pct Recovery = 100% Analysis Date = 10/05/17 Pct Recovery = 100% Analysis Date = 09/25/17 Pct Recovery = 100% Analysis Date = 09/25/17 Pct Recovery = 100% Analysis Date = 09/15/17 Pct Recovery = 100% Analysis Date = 09/15/17 Pct Recovery = 100% Analysis Date = 09/05/17 Pct Recovery = 100% Analysis Date = 09/05/17 Pct Recovery = 100% Analysis Date = 08/26/17 Pct Recovery = 99% Analysis Date = 08/26/17 Pct Recovery = 99% Analysis Date = 08/16/17 Pct Recovery = 99% Analysis Date = 08/16/17 Pct Recovery = 99% Analysis Date = 08/06/17 Pct Recovery = 99% Analysis Date = 08/06/17 Pct Recovery = 99% Analysis Date = 07/27/17 Pct Recovery = 99% Analysis Date = 07/27/17 Pct Recovery = 99% Analysis Date = 07/18/17 Pct Recovery = 99% Analysis Date = 07/18/17 Pct Recovery = 99% Analysis Date = 07/08/17 Pct Recovery = 98% Analysis Date = 07/08/17 Pct Recovery = 98% Analysis Date = 06/28/17 Pct Recovery = 98% Analysis Date = 06/28/17 Pct Recovery = 98% Analysis Date = 06/18/17 Pct Recovery = 98% Analysis Date = 06/18/17 Pct Recovery = 98% Analysis Date = 06/08/17 Pct Recovery = 98% Analysis Date = 06/08/17 Pct Recovery = 98% Analysis Date = 05/29/17 Pct Recovery = 97% Analysis Date = 05/29/17 Pct Recovery = 97% Analysis Date = 05/19/17 Pct Recovery = 97% Analysis Date = 05/19/17 Pct Recovery = 97% Analysis Date = 05/09/17 Pct Recovery = 97% Analysis Date = 05/09/17 Pct Recovery = 97% Analysis Date = 04/29/17 Pct Recovery = 97% Analysis Date = 04/29/17 Pct Recovery = 97% Analysis Date = 04/19/17 Pct Recovery = 97% Analysis Date = 04/19/17 Pct Recovery = 97% Analysis Date = 04/09/17 Pct Recovery = 96% Analysis Date = 04/09/17 Pct Recovery = 96% Analysis Date = 03/31/17 Pct Recovery = 96% Analysis Date = 03/31/17 Pct Recovery = 96% Analysis Date = 03/21/17 Pct Recovery = 96% Analysis Date = 03/21/17 Pct Recovery = 96% Analysis Date = 03/11/17 Pct Recovery = 96% Analysis Date = 03/11/17 Pct Recovery = 96% Analysis Date = 03/01/17 Pct Recovery = 96% Analysis Date = 03/01/17 Pct Recovery = 96% Analysis Date = 02/19/17 Pct Recovery = 95% Analysis Date = 02/19/17 Pct Recovery = 95% Analysis Date = 02/09/17 Pct Recovery = 95% Analysis Date = 02/09/17 Pct Recovery = 95% Analysis Date = 01/30/17 Pct Recovery = 95% Analysis Date = 01/30/17 Pct Recovery = 95% Analysis Date = 01/20/17 Pct Recovery = 95% Analysis Date = 01/20/17 Pct Recovery = 95% Analysis Date = 01/10/17 Pct Recovery = 95% Analysis Date = 01/10/17 Pct Recovery = 95% Analysis Date = 12/31/16 Pct Recovery = 94% Analysis Date = 12/31/16 Pct Recovery = 94% Analysis Date = 12/21/16 Pct Recovery = 94% Analysis Date = 12/21/16 Pct Recovery = 94% Analysis Date = 12/12/16 Pct Recovery = 94% Analysis Date = 12/12/16 Pct Recovery = 94% Analysis Date = 12/02/16 Pct Recovery = 94% Analysis Date = 12/02/16 Pct Recovery = 94% Analysis Date = 11/22/16 Pct Recovery = 94% Analysis Date = 11/22/16 Pct Recovery = 94% Analysis Date = 11/12/16 Pct Recovery = 93% Analysis Date = 11/12/16 Pct Recovery = 93% Analysis Date = 11/02/16 Pct Recovery = 93% Analysis Date = 11/02/16 Pct Recovery = 93% Analysis Date = 10/23/16 Pct Recovery = 93% Analysis Date = 10/23/16 Pct Recovery = 93% Analysis Date = 10/13/16 Pct Recovery = 93% Analysis Date = 10/13/16 Pct Recovery = 93% Analysis Date = 10/03/16 Pct Recovery = 92% Analysis Date = 10/03/16 Pct Recovery = 92% Analysis Date = 09/23/16 Pct Recovery = 92% Analysis Date = 09/23/16 Pct Recovery = 92% Analysis Date = 09/13/16 Pct Recovery = 92% Analysis Date = 09/13/16 Pct Recovery = 92% Analysis Date = 09/03/16 Pct Recovery = 92% Analysis Date = 09/03/16 Pct Recovery = 92% Analysis Date = 08/25/16 Pct Recovery = 92% Analysis Date = 08/25/16 Pct Recovery = 92% Analysis Date = 08/15/16 Pct Recovery = 92% Analysis Date = 08/15/16 Pct Recovery = 92% Analysis Date = 08/05/16 Pct Recovery = 92% Analysis Date = 08/05/16 Pct Recovery = 92% Analysis Date = 07/26/16 Pct Recovery = 92% Analysis Date = 07/26/16 Pct Recovery = 92% Analysis Date = 07/16/16 Pct Recovery = 92% Analysis Date = 07/16/16 Pct Recovery = 92% Analysis Date = 07/06/16 Pct Recovery = 92% Analysis Date = 07/06/16 Pct Recovery = 92% Analysis Date = 06/26/16 Pct Recovery = 92% Analysis Date = 06/26/16 Pct Recovery = 92% Analysis Date = 06/16/16 Pct Recovery = 92% Analysis Date = 06/16/16 Pct Recovery = 92% Analysis Date = 06/06/16 Pct Recovery = 92% Analysis Date = 06/06/16 Pct Recovery = 92% Analysis Date = 05/27/16 Pct Recovery = 92% Analysis Date = 05/27/16 Pct Recovery = 92% Analysis Date = 05/17/16 Pct Recovery = 92% Analysis Date = 05/17/16 Pct Recovery = 92% Analysis Date = 05/08/16 Pct Recovery = 92% Analysis Date = 05/08/16 Pct Recovery = 92% Analysis Date = 04/28/16 Pct Recovery = 92% Analysis Date = 04/28/16 Pct Recovery = 92% Analysis Date = 04/18/16 Pct Recovery = 92% Analysis Date = 04/18/16 Pct Recovery = 92% Analysis Date = 04/08/16 Pct Recovery = 92% Analysis Date = 04/08/16 Pct Recovery = 92% Analysis Date = 03/29/16 Pct Recovery = 92% Analysis Date = 03/29/16 Pct Recovery = 92% Analysis Date = 03/19/16 Pct Recovery = 92% Analysis Date = 03/19/16 Pct Recovery = 92% Analysis Date = 03/09/16 Pct Recovery = 92% Analysis Date = 03/09/16 Pct Recovery = 92% Analysis Date = 02/28/16 Pct Recovery = 92% Analysis Date = 02/28/16 Pct Recovery = 92% Analysis Date = 02/18/16 Pct Recovery = 92% Analysis Date = 02/18/16 Pct Recovery = 92% Analysis Date = 02/08/16 Pct Recovery = 92% Analysis Date = 02/08/16 Pct Recovery = 92% Analysis Date = 01/29/16 Pct Recovery = 92% Analysis Date = 01/29/16 Pct Recovery = 92% Analysis Date = 01/20/16 Pct Recovery = 92% Analysis Date = 01/20/16 Pct Recovery = 92% Analysis Date = 01/10/16 Pct Recovery = 92% Analysis Date = 01/10/16 Pct Recovery = 92% Analysis Date = 12/31/15 Pct Recovery = 92% Analysis Date = 12/31/15 Pct Recovery = 92% Analysis Date = 12/21/15 Pct Recovery = 92% Analysis Date = 12/21/15 Pct Recovery = 92% Analysis Date = 12/11/15 Pct Recovery = 92% Analysis Date = 12/11/15 Pct Recovery = 92% Analysis Date = 12/01/15 Pct Recovery = 92% Analysis Date = 12/01/15 Pct Recovery = 92% Analysis Date = 11/21/15 Pct Recovery = 92% Analysis Date = 11/21/15 Pct Recovery = 92% Analysis Date = 11/11/15 Pct Recovery = 92% Analysis Date = 11/11/15 Pct Recovery = 92% Analysis Date = 11/01/15 Pct Recovery = 92% Analysis Date = 11/01/15 Pct Recovery = 92% Analysis Date = 10/22/15 Pct Recovery = 92% Analysis Date = 10/22/15 Pct Recovery = 92% Analysis Date = 10/12/15 Pct Recovery = 92% Analysis Date = 10/12/15 Pct Recovery = 92% Analysis Date = 10/02/15 Pct Recovery = 91% Analysis Date = 10/02/15 Pct Recovery = 91% Analysis Date = 09/23/15 Pct Recovery = 91% Analysis Date = 09/23/15 Pct Recovery = 91% Analysis Date = 09/13/15 Pct Recovery = 91% Analysis Date = 09/13/15 Pct Recovery = 91% Analysis Date = 09/03/15 Pct Recovery = 91% Analysis Date = 09/03/15 Pct Recovery = 91% Analysis Date = 08/24/15 Pct Recovery = 91% Analysis Date = 08/24/15 Pct Recovery = 91% Analysis Date = 08/14/15 Pct Recovery = 91% Analysis Date = 08/14/15 Pct Recovery = 91% Analysis Date = 08/04/15 Pct Recovery = 91% Analysis Date = 08/04/15 Pct Recovery = 91% Analysis Date = 07/25/15 Pct Recovery = 91% Analysis Date = 07/25/15 Pct Recovery = 91% Analysis Date = 07/15/15 Pct Recovery = 91% Analysis Date = 07/15/15 Pct Recovery = 91% Analysis Date = 07/05/15 Pct Recovery = 91% Analysis Date = 07/05/15 Pct Recovery = 91% Analysis Date = 06/25/15 Pct Recovery = 91% Analysis Date = 06/25/15 Pct Recovery = 91% Analysis Date = 06/15/15 Pct Recovery = 91% Analysis Date = 06/15/15 Pct Recovery = 91% Analysis Date = 06/06/15 Pct Recovery = 91% Analysis Date = 06/06/15 Pct Recovery = 91% Analysis Date = 05/27/15 Pct Recovery = 91% Analysis Date = 05/27/15 Pct Recovery = 91% Analysis Date = 05/17/15 Pct Recovery = 91% Analysis Date = 05/17/15 Pct Recovery = 91% Analysis Date = 05/07/15 Pct Recovery = 91% Analysis Date = 05/07/15 Pct Recovery = 91% Analysis Date = 04/27/15 Pct Recovery = 91% Analysis Date = 04/27/15 Pct Recovery = 91% Analysis Date = 04/17/15 Pct Recovery = 91% Analysis Date = 04/17/15 Pct Recovery = 91% Analysis Date = 04/07/15 Pct Recovery = 91% Analysis Date = 04/07/15 Pct Recovery = 91% Analysis Date = 03/28/15 Pct Recovery = 90% Analysis Date = 03/28/15 Pct Recovery = 90% Analysis Date = 03/18/15 Pct Recovery = 90% Analysis Date = 03/18/15 Pct Recovery = 90% Analysis Date = 03/08/15 Pct Recovery = 90% Analysis Date = 03/08/15 Pct Recovery = 90% Analysis Date = 02/26/15 Pct Recovery = 90% Analysis Date = 02/26/15 Pct Recovery = 90% Analysis Date = 02/17/15 Pct Recovery = 90% Analysis Date = 02/17/15 Pct Recovery = 90% Analysis Date = 02/07/15 Pct Recovery = 90% Analysis Date = 02/07/15 Pct Recovery = 90% Analysis Date = 01/28/15 Pct Recovery = 90% Analysis Date = 01/28/15 Pct Recovery = 90% Analysis Date = 01/18/15 Pct Recovery = 90% Analysis Date = 01/18/15 Pct Recovery = 90% Analysis Date = 01/08/15 Pct Recovery = 90% Analysis Date = 01/08/15 Pct Recovery = 90% Analysis Date = 12/29/14 Pct Recovery = 90% Analysis Date = 12/29/14 Pct Recovery = 90% Analysis Date = 12/19/14 Pct Recovery = 90% Analysis Date = 12/19/14 Pct Recovery = 90% Analysis Date = 12/09/14 Pct Recovery = 90% Analysis Date = 12/09/14 Pct Recovery = 90% Analysis Date = 11/29/14 Pct Recovery = 90% Analysis Date = 11/29/14 Pct Recovery = 90% Analysis Date = 11/19/14 Pct Recovery = 90% Analysis Date = 11/19/14 Pct Recovery = 90% Analysis Date = 11/09/14 Pct Recovery = 90% Analysis Date = 11/09/14 Pct Recovery = 90% Analysis Date = 10/31/14 Pct Recovery = 90% Analysis Date = 10/31/14 Pct Recovery = 90% Analysis Date = 10/21/14 Pct Recovery = 90% Analysis Date = 10/21/14 Pct Recovery = 90% Analysis Date = 10/11/14 Pct Recovery = 90% Analysis Date = 10/11/14 Pct Recovery = 90% Analysis Date = 10/01/14 Pct Recovery = 90% Analysis Date = 10/01/14 Pct Recovery = 90% Analysis Date = 09/21/14 Pct Recovery = 89% Analysis Date = 09/21/14 Pct Recovery = 89% Analysis Date = 09/11/14 Pct Recovery = 89% Analysis Date = 09/11/14 Pct Recovery = 89% Analysis Date = 09/01/14 Pct Recovery = 89% Analysis Date = 09/01/14 Pct Recovery = 89% Analysis Date = 08/22/14 Pct Recovery = 89% Analysis Date = 08/22/14 Pct Recovery = 89% Analysis Date = 08/12/14 Pct Recovery = 89% Analysis Date = 08/12/14 Pct Recovery = 89% Analysis Date = 08/02/14 Pct Recovery = 89% Analysis Date = 08/02/14 Pct Recovery = 89% Analysis Date = 07/23/14 Pct Recovery = 89% Analysis Date = 07/23/14 Pct Recovery = 89% Analysis Date = 07/14/14 Pct Recovery = 89% Analysis Date = 07/14/14 Pct Recovery = 89% Analysis Date = 07/04/14 Pct Recovery = 89% Analysis Date = 07/04/14 Pct Recovery = 89% Analysis Date = 06/24/14 Pct Recovery = 88% Analysis Date = 06/24/14 Pct Recovery = 88% Analysis Date = 06/14/14 Pct Recovery = 88% Analysis Date = 06/14/14 Pct Recovery = 88% Analysis Date = 06/04/14 Pct Recovery = 88% Analysis Date = 06/04/14 Pct Recovery = 88% Analysis Date = 05/25/14 Pct Recovery = 88% Analysis Date = 05/25/14 Pct Recovery = 88% Analysis Date = 05/15/14 Pct Recovery = 88% Analysis Date = 05/15/14 Pct Recovery = 88% Analysis Date = 05/05/14 Pct Recovery = 88% Analysis Date = 05/05/14 Pct Recovery = 88% Analysis Date = 04/25/14 Pct Recovery = 88% Analysis Date = 04/25/14 Pct Recovery = 88% Analysis Date = 04/15/14 Pct Recovery = 88% Analysis Date = 04/15/14 Pct Recovery = 88% Analysis Date = 04/05/14 Pct Recovery = 88% Analysis Date = 04/05/14 Pct Recovery = 88% Analysis Date = 03/27/14 Pct Recovery = 88% Analysis Date = 03/27/14 Pct Recovery = 88% Analysis Date = 03/17/14 Pct Recovery = 88% Analysis Date = 03/17/14 Pct Recovery = 88% Analysis Date = 03/07/14 Pct Recovery = 88% Analysis Date = 03/07/14 Pct Recovery = 88% Analysis Date = 02/25/14 Pct Recovery = 88% Analysis Date = 02/25/14 Pct Recovery = 88% Analysis Date = 02/15/14 Pct Recovery = 88% Analysis Date = 02/15/14 Pct Recovery = 88% Analysis Date = 02/05/14 Pct Recovery = 88% Analysis Date = 02/05/14 Pct Recovery = 88% Analysis Date = 01/26/14 Pct Recovery = 88% Analysis Date = 01/26/14 Pct Recovery = 88% Analysis Date = 01/16/14 Pct Recovery = 88% Analysis Date = 01/16/14 Pct Recovery = 88% Analysis Date = 01/06/14 Pct Recovery = 88% Analysis Date = 01/06/14 Pct Recovery = 88% Analysis Date = 12/27/13 Pct Recovery = 88% Analysis Date = 12/27/13 Pct Recovery = 88% Analysis Date = 12/17/13 Pct Recovery = 88% Analysis Date = 12/17/13 Pct Recovery = 88% Analysis Date = 12/08/13 Pct Recovery = 88% Analysis Date = 12/08/13 Pct Recovery = 88% Analysis Date = 11/28/13 Pct Recovery = 88% Analysis Date = 11/28/13 Pct Recovery = 88% Analysis Date = 11/18/13 Pct Recovery = 88% Analysis Date = 11/18/13 Pct Recovery = 88% Analysis Date = 11/08/13 Pct Recovery = 88% Analysis Date = 11/08/13 Pct Recovery = 88% Analysis Date = 10/29/13 Pct Recovery = 88% Analysis Date = 10/29/13 Pct Recovery = 88% Analysis Date = 10/19/13 Pct Recovery = 88% Analysis Date = 10/19/13 Pct Recovery = 88% Analysis Date = 10/09/13 Pct Recovery = 88% Analysis Date = 10/09/13 Pct Recovery = 88% Analysis Date = 09/29/13 Pct Recovery = 88% Analysis Date = 09/29/13 Pct Recovery = 88% Analysis Date = 09/19/13 Pct Recovery = 87% Analysis Date = 09/19/13 Pct Recovery = 87% Analysis Date = 09/09/13 Pct Recovery = 87% Analysis Date = 09/09/13 Pct Recovery = 87% Analysis Date = 08/30/13 Pct Recovery = 87% Analysis Date = 08/30/13 Pct Recovery = 87% Analysis Date = 08/21/13 Pct Recovery = 87% Analysis Date = 08/21/13 Pct Recovery = 87% Analysis Date = 08/11/13 Pct Recovery = 87% Analysis Date = 08/11/13 Pct Recovery = 87% Analysis Date = 08/01/13 Pct Recovery = 87% Analysis Date = 08/01/13 Pct Recovery = 87% Analysis Date = 07/22/13 Pct Recovery = 87% Analysis Date = 07/22/13 Pct Recovery = 87% Analysis Date = 07/12/13 Pct Recovery = 87% Analysis Date = 07/12/13 Pct Recovery = 87% Analysis Date = 07/02/13 Pct Recovery = 87% Analysis Date = 07/02/13 Pct Recovery = 87% Analysis Date = 06/22/13 Pct Recovery = 87% Analysis Date = 06/22/13 Pct Recovery = 87% Analysis Date = 06/12/13 Pct Recovery = 87% Analysis Date = 06/12/13 Pct Recovery = 87% Analysis Date = 06/02/13 Pct Recovery = 87% Analysis Date = 06/02/13 Pct Recovery = 87% Analysis Date = 05/23/13 Pct Recovery = 87% Analysis Date = 05/23/13 Pct Recovery = 87% Analysis Date = 05/13/13 Pct Recovery = 87% Analysis Date = 05/13/13 Pct Recovery = 87% Analysis Date = 05/04/13 Pct Recovery = 87% Analysis Date = 05/04/13 Pct Recovery = 87% Analysis Date = 04/24/13 Pct Recovery = 87% Analysis Date = 04/24/13 Pct Recovery = 87% Analysis Date = 04/14/13 Pct Recovery = 87% Analysis Date = 04/14/13 Pct Recovery = 87% Analysis Date = 04/04/13 Pct Recovery = 87% Analysis Date = 04/04/13 Pct Recovery = 87% Analysis Date = 03/25/13 Pct Recovery = 87% Analysis Date = 03/25/13 Pct Recovery = 87% Analysis Date = 03/15/13 Pct Recovery = 87% Analysis Date = 03/15/13 Pct Recovery = 87% Analysis Date = 03/05/13 Pct Recovery = 87% Analysis Date = 03/05/13 Pct Recovery = 87% Analysis Date = 02/23/13 Pct Recovery = 87% Analysis Date = 02/23/13 Pct Recovery = 87% Analysis Date = 02/13/13 Pct Recovery = 87% Analysis Date = 02/13/13 Pct Recovery = 87% Analysis Date = 02/03/13 Pct Recovery = 87% Analysis Date = 02/03/13 Pct Recovery = 87% Analysis Date = 01/24/13 Pct Recovery = 87% Analysis Date = 01/24/13 Pct Recovery = 87% Analysis Date = 01/15/13 Pct Recovery = 87% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
PENDIMETHALIN

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 73 92% 16% 88% 13%
Total 73 92% 16% 88% 13%

Sample Statistics
PENDIMETHALIN

Characteristic N % % Basis
Plotted 73 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 73 .  
False Negatives 0 0% 0 out of 73
Not Spiked 61 .  
False Positives 0 0% 0 out of 61

OBSP Determination:
PHORATE
METHOD: 2033 , TESTIDCODE: 82664GCM35

Laboratory ID = 20130250061 Lab Value = 0.175 Expected Conc. = 0.293 Report level label = 0.02 Pct Recovery = 60% Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl SpecificMix = 05BB029 Laboratory ID = 20140100085 Lab Value = 0.198 Expected Conc. = 0.216 Report level label = 0.02 Pct Recovery = 92% Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl SpecificMix = 042413 Laboratory ID = 20130940097 Lab Value = 0.041 Expected Conc. = 0.1515 Report level label = 0.02 Pct Recovery = 27% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = 052412 Laboratory ID = 20130100066 Lab Value = 0.080 Expected Conc. = 0.1515 Report level label = 0.02 Pct Recovery = 53% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl SpecificMix = 052412 Laboratory ID = 20140230082 Lab Value = 0.113 Expected Conc. = 0.1505 Report level label = 0.02 Pct Recovery = 75% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl SpecificMix = 012513 Laboratory ID = 20132420001 Lab Value = 0.104 Expected Conc. = 0.1505 Report level label = 0.02 Pct Recovery = 69% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl SpecificMix = 012513 Laboratory ID = 20172510330 Lab Value = 0.100 Expected Conc. = 0.134 Report level label = 0.02 Pct Recovery = 75% Analysis Date = 12/29/17 SpikeMix = ChemService 6537100: 100 µl & Abs 071817Pest: 100 µl SpecificMix = 071817Pest Laboratory ID = 20163370001 Lab Value = 0.102 Expected Conc. = 0.125 Report level label = 0.02 Pct Recovery = 82% Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl SpecificMix = B20160331 Laboratory ID = 20163150006 Lab Value = 0.095 Expected Conc. = 0.125 Report level label = 0.02 Pct Recovery = 76% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl SpecificMix = B20160331 Laboratory ID = 20161880109 Lab Value = 0.131 Expected Conc. = 0.122 Report level label = 0.02 Pct Recovery = 107% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl SpecificMix = 03FF076 Laboratory ID = 20132690010 Lab Value = 0.122 Expected Conc. = 0.108 Report level label = 0.02 Pct Recovery = 113% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl SpecificMix = 042413 Laboratory ID = 20132560001 Lab Value = 0.090 Expected Conc. = 0.108 Report level label = 0.02 Pct Recovery = 83% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl SpecificMix = 042413 Laboratory ID = 20132140002 Lab Value = 0.027 Expected Conc. = 0.105 Report level label = 0.02 Pct Recovery = 26% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl SpecificMix = 04CC101 Laboratory ID = 20171720140 Lab Value = 0.104 Expected Conc. = 0.1 Report level label = 0.02 Pct Recovery = 104% Analysis Date = 08/31/17 SpikeMix = Supelco LC20138V: 80 µl & Phenova B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20171660002 Lab Value = 0.105 Expected Conc. = 0.1 Report level label = 0.02 Pct Recovery = 105% Analysis Date = 08/23/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20170190026 Lab Value = 0.079 Expected Conc. = 0.1 Report level label = 0.02 Pct Recovery = 79% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20161470001 Lab Value = 0.088 Expected Conc. = 0.1 Report level label = 0.02 Pct Recovery = 88% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20170960001 Lab Value = 0.069 Expected Conc. = 0.0976 Report level label = 0.02 Pct Recovery = 71% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl SpecificMix = 03FF076 Laboratory ID = 20150720069 Lab Value = 0.027 Expected Conc. = 0.081 Report level label = 0.02 Pct Recovery = 33% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 0227-14-08 Laboratory ID = 20141770149 Lab Value = 0.054 Expected Conc. = 0.081 Report level label = 0.02 Pct Recovery = 67% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl SpecificMix = 0227-14-08 Laboratory ID = 20141570088 Lab Value = 0.045 Expected Conc. = 0.081 Report level label = 0.02 Pct Recovery = 56% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl SpecificMix = 0227-14-08 Laboratory ID = 20181430122 Lab Value = 0.051 Expected Conc. = 0.067 Report level label = 0.02 Pct Recovery = 76% Analysis Date = 06/20/18 SpikeMix = Abs 071817Pest: 50 µl & Spex Organics EN170808006: 50 µl SpecificMix = 071817Pest Laboratory ID = 20173480003 Lab Value = 0.054 Expected Conc. = 0.065 Report level label = 0.02 Pct Recovery = 83% Analysis Date = 04/05/18 SpikeMix = Abs 071717Pest: 50 µl & ChemService 6567600: 50 µl SpecificMix = 6567600 Laboratory ID = 20172560101 Lab Value = 0.039 Expected Conc. = 0.065 Report level label = 0.02 Pct Recovery = 60% Analysis Date = 12/22/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6567600: 50 µl SpecificMix = 6567600 Laboratory ID = 20133400002 Lab Value = 0.045 Expected Conc. = 0.0606 Report level label = 0.02 Pct Recovery = 74% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = 052412 Laboratory ID = 20132910008 Lab Value = 0.043 Expected Conc. = 0.0606 Report level label = 0.02 Pct Recovery = 71% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = 052412 Laboratory ID = 20130650005 Lab Value = 0.027 Expected Conc. = 0.0606 Report level label = 0.02 Pct Recovery = 45% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl SpecificMix = 052412 Laboratory ID = 20140860102 Lab Value = 0.023 Expected Conc. = 0.0602 Report level label = 0.02 Pct Recovery = 38% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 012513 Laboratory ID = 20131920149 Lab Value = 0.029 Expected Conc. = 0.0602 Report level label = 0.02 Pct Recovery = 48% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl SpecificMix = 012513 Laboratory ID = 20161260151 Lab Value = 0.042 Expected Conc. = 0.06 Report level label = 0.02 Pct Recovery = 70% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = 3851600 Laboratory ID = 20160770090 Lab Value = 0.033 Expected Conc. = 0.06 Report level label = 0.02 Pct Recovery = 55% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20160630046 Lab Value = 0.026 Expected Conc. = 0.06 Report level label = 0.02 Pct Recovery = 43% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20153510109 Lab Value = 0.034 Expected Conc. = 0.06 Report level label = 0.02 Pct Recovery = 57% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20153440001 Lab Value = 0.031 Expected Conc. = 0.06 Report level label = 0.02 Pct Recovery = 52% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20151270112 Lab Value = 0.048 Expected Conc. = 0.06 Report level label = 0.02 Pct Recovery = 80% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl SpecificMix = 3851600 Laboratory ID = 20130510051 Lab Value = 0.013 Expected Conc. = 0.0586 Report level label = 0.02 Pct Recovery = 22% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl SpecificMix = 05BB029 Laboratory ID = 20171160110 Lab Value = 0.036 Expected Conc. = 0.05 Report level label = 0.02 Pct Recovery = 72% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = B20160331 Laboratory ID = 20162380004 Lab Value = 0.039 Expected Conc. = 0.05 Report level label = 0.02 Pct Recovery = 78% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = B20160331 Laboratory ID = 20162150213 Lab Value = 0.040 Expected Conc. = 0.05 Report level label = 0.02 Pct Recovery = 80% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl SpecificMix = B20160331 Laboratory ID = 20172020035 Lab Value = 0.040 Expected Conc. = 0.0488 Report level label = 0.02 Pct Recovery = 82% Analysis Date = 11/07/17 SpikeMix = Abs 071717Pest: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20171510080 Lab Value = 0.041 Expected Conc. = 0.0488 Report level label = 0.02 Pct Recovery = 84% Analysis Date = 06/09/17 SpikeMix = Supelco LC20138V: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20170460061 Lab Value = 0.028 Expected Conc. = 0.0488 Report level label = 0.02 Pct Recovery = 57% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl SpecificMix = 03FF076 Laboratory ID = 20162660005 Lab Value = 0.028 Expected Conc. = 0.0488 Report level label = 0.02 Pct Recovery = 57% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl SpecificMix = 03FF076 Laboratory ID = 20161600087 Lab Value = 0.038 Expected Conc. = 0.0488 Report level label = 0.02 Pct Recovery = 78% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20161340228 Lab Value = 0.031 Expected Conc. = 0.0488 Report level label = 0.02 Pct Recovery = 64% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl SpecificMix = 03FF076 Laboratory ID = 20161190075 Lab Value = 0.028 Expected Conc. = 0.0488 Report level label = 0.02 Pct Recovery = 57% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20133580036 Lab Value = 0.017 Expected Conc. = 0.0432 Report level label = 0.02 Pct Recovery = 39% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 042413 Laboratory ID = 20133190012 Lab Value = 0.032 Expected Conc. = 0.0432 Report level label = 0.02 Pct Recovery = 74% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 042413 Laboratory ID = 20131650073 Lab Value = 0.018 Expected Conc. = 0.0432 Report level label = 0.02 Pct Recovery = 42% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl SpecificMix = 042413 Laboratory ID = 20140730138 Lab Value = 0.029 Expected Conc. = 0.042 Report level label = 0.02 Pct Recovery = 69% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 04CC101 Laboratory ID = 20140510043 Lab Value = 0.016 Expected Conc. = 0.042 Report level label = 0.02 Pct Recovery = 38% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 04CC101 Laboratory ID = 20133310030 Lab Value = 0.034 Expected Conc. = 0.042 Report level label = 0.02 Pct Recovery = 81% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl SpecificMix = 04CC101 Laboratory ID = 20132280016 Lab Value = 0.024 Expected Conc. = 0.042 Report level label = 0.02 Pct Recovery = 57% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl SpecificMix = 04CC101 Laboratory ID = 20141840097 Lab Value = 0.012 Expected Conc. = 0.0405 Report level label = 0.02 Pct Recovery = 30% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20141490205 Lab Value = 0.034 Expected Conc. = 0.0405 Report level label = 0.02 Pct Recovery = 84% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20141420140 Lab Value = 0.013 Expected Conc. = 0.0405 Report level label = 0.02 Pct Recovery = 32% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20141360094 Lab Value = 0.021 Expected Conc. = 0.0405 Report level label = 0.02 Pct Recovery = 52% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20180730064 Lab Value = 0.034 Expected Conc. = 0.0402 Report level label = 0.02 Pct Recovery = 85% Analysis Date = 05/16/18 SpikeMix = Abs 071717Pest: 30 µl & Abs 071817Pest: 30 µl SpecificMix = 071817Pest Laboratory ID = 20180050004 Lab Value = 0.029 Expected Conc. = 0.0402 Report level label = 0.02 Pct Recovery = 72% Analysis Date = 04/05/18 SpikeMix = Abs 071817Pest: 30 µl & ChemService 6472100: 30 µl SpecificMix = 071817Pest Laboratory ID = 20160430111 Lab Value = 0.019 Expected Conc. = 0.03 Report level label = 0.02 Pct Recovery = 63% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 3851600 Laboratory ID = 20160210080 Lab Value = 0.015 Expected Conc. = 0.03 Report level label = 0.02 Pct Recovery = 50% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 3851600 Laboratory ID = 20152950078 Lab Value = 0.012 Expected Conc. = 0.03 Report level label = 0.02 Pct Recovery = 40% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 3851600 Laboratory ID = 20153030068 Lab Value = 0.019 Expected Conc. = 0.03 Report level label = 0.02 Pct Recovery = 63% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = 3851600 Analysis Date = 06/20/18 Pct Recovery = 85% Analysis Date = 06/10/18 Pct Recovery = 85% Analysis Date = 06/10/18 Pct Recovery = 85% Analysis Date = 05/31/18 Pct Recovery = 85% Analysis Date = 05/31/18 Pct Recovery = 85% Analysis Date = 05/21/18 Pct Recovery = 85% Analysis Date = 05/21/18 Pct Recovery = 85% Analysis Date = 05/11/18 Pct Recovery = 85% Analysis Date = 05/11/18 Pct Recovery = 85% Analysis Date = 05/01/18 Pct Recovery = 84% Analysis Date = 05/01/18 Pct Recovery = 84% Analysis Date = 04/21/18 Pct Recovery = 84% Analysis Date = 04/21/18 Pct Recovery = 84% Analysis Date = 04/11/18 Pct Recovery = 84% Analysis Date = 04/11/18 Pct Recovery = 84% Analysis Date = 04/01/18 Pct Recovery = 84% Analysis Date = 04/01/18 Pct Recovery = 84% Analysis Date = 03/22/18 Pct Recovery = 83% Analysis Date = 03/22/18 Pct Recovery = 83% Analysis Date = 03/13/18 Pct Recovery = 83% Analysis Date = 03/13/18 Pct Recovery = 83% Analysis Date = 03/03/18 Pct Recovery = 83% Analysis Date = 03/03/18 Pct Recovery = 83% Analysis Date = 02/21/18 Pct Recovery = 83% Analysis Date = 02/21/18 Pct Recovery = 83% Analysis Date = 02/11/18 Pct Recovery = 82% Analysis Date = 02/11/18 Pct Recovery = 82% Analysis Date = 02/01/18 Pct Recovery = 82% Analysis Date = 02/01/18 Pct Recovery = 82% Analysis Date = 01/22/18 Pct Recovery = 82% Analysis Date = 01/22/18 Pct Recovery = 82% Analysis Date = 01/12/18 Pct Recovery = 82% Analysis Date = 01/12/18 Pct Recovery = 82% Analysis Date = 01/02/18 Pct Recovery = 81% Analysis Date = 01/02/18 Pct Recovery = 81% Analysis Date = 12/23/17 Pct Recovery = 81% Analysis Date = 12/23/17 Pct Recovery = 81% Analysis Date = 12/13/17 Pct Recovery = 81% Analysis Date = 12/13/17 Pct Recovery = 81% Analysis Date = 12/04/17 Pct Recovery = 81% Analysis Date = 12/04/17 Pct Recovery = 81% Analysis Date = 11/24/17 Pct Recovery = 80% Analysis Date = 11/24/17 Pct Recovery = 80% Analysis Date = 11/14/17 Pct Recovery = 80% Analysis Date = 11/14/17 Pct Recovery = 80% Analysis Date = 11/04/17 Pct Recovery = 80% Analysis Date = 11/04/17 Pct Recovery = 80% Analysis Date = 10/25/17 Pct Recovery = 80% Analysis Date = 10/25/17 Pct Recovery = 80% Analysis Date = 10/15/17 Pct Recovery = 80% Analysis Date = 10/15/17 Pct Recovery = 80% Analysis Date = 10/05/17 Pct Recovery = 79% Analysis Date = 10/05/17 Pct Recovery = 79% Analysis Date = 09/25/17 Pct Recovery = 79% Analysis Date = 09/25/17 Pct Recovery = 79% Analysis Date = 09/15/17 Pct Recovery = 79% Analysis Date = 09/15/17 Pct Recovery = 79% Analysis Date = 09/05/17 Pct Recovery = 79% Analysis Date = 09/05/17 Pct Recovery = 79% Analysis Date = 08/27/17 Pct Recovery = 78% Analysis Date = 08/27/17 Pct Recovery = 78% Analysis Date = 08/17/17 Pct Recovery = 78% Analysis Date = 08/17/17 Pct Recovery = 78% Analysis Date = 08/07/17 Pct Recovery = 78% Analysis Date = 08/07/17 Pct Recovery = 78% Analysis Date = 07/28/17 Pct Recovery = 78% Analysis Date = 07/28/17 Pct Recovery = 78% Analysis Date = 07/18/17 Pct Recovery = 77% Analysis Date = 07/18/17 Pct Recovery = 77% Analysis Date = 07/08/17 Pct Recovery = 77% Analysis Date = 07/08/17 Pct Recovery = 77% Analysis Date = 06/28/17 Pct Recovery = 77% Analysis Date = 06/28/17 Pct Recovery = 77% Analysis Date = 06/18/17 Pct Recovery = 77% Analysis Date = 06/18/17 Pct Recovery = 77% Analysis Date = 06/08/17 Pct Recovery = 76% Analysis Date = 06/08/17 Pct Recovery = 76% Analysis Date = 05/29/17 Pct Recovery = 76% Analysis Date = 05/29/17 Pct Recovery = 76% Analysis Date = 05/20/17 Pct Recovery = 76% Analysis Date = 05/20/17 Pct Recovery = 76% Analysis Date = 05/10/17 Pct Recovery = 75% Analysis Date = 05/10/17 Pct Recovery = 75% Analysis Date = 04/30/17 Pct Recovery = 75% Analysis Date = 04/30/17 Pct Recovery = 75% Analysis Date = 04/20/17 Pct Recovery = 75% Analysis Date = 04/20/17 Pct Recovery = 75% Analysis Date = 04/10/17 Pct Recovery = 75% Analysis Date = 04/10/17 Pct Recovery = 75% Analysis Date = 03/31/17 Pct Recovery = 74% Analysis Date = 03/31/17 Pct Recovery = 74% Analysis Date = 03/21/17 Pct Recovery = 74% Analysis Date = 03/21/17 Pct Recovery = 74% Analysis Date = 03/11/17 Pct Recovery = 74% Analysis Date = 03/11/17 Pct Recovery = 74% Analysis Date = 03/01/17 Pct Recovery = 74% Analysis Date = 03/01/17 Pct Recovery = 74% Analysis Date = 02/19/17 Pct Recovery = 73% Analysis Date = 02/19/17 Pct Recovery = 73% Analysis Date = 02/10/17 Pct Recovery = 73% Analysis Date = 02/10/17 Pct Recovery = 73% Analysis Date = 01/31/17 Pct Recovery = 73% Analysis Date = 01/31/17 Pct Recovery = 73% Analysis Date = 01/21/17 Pct Recovery = 73% Analysis Date = 01/21/17 Pct Recovery = 73% Analysis Date = 01/11/17 Pct Recovery = 72% Analysis Date = 01/11/17 Pct Recovery = 72% Analysis Date = 01/01/17 Pct Recovery = 72% Analysis Date = 01/01/17 Pct Recovery = 72% Analysis Date = 12/22/16 Pct Recovery = 72% Analysis Date = 12/22/16 Pct Recovery = 72% Analysis Date = 12/12/16 Pct Recovery = 71% Analysis Date = 12/12/16 Pct Recovery = 71% Analysis Date = 12/02/16 Pct Recovery = 71% Analysis Date = 12/02/16 Pct Recovery = 71% Analysis Date = 11/22/16 Pct Recovery = 71% Analysis Date = 11/22/16 Pct Recovery = 71% Analysis Date = 11/12/16 Pct Recovery = 70% Analysis Date = 11/12/16 Pct Recovery = 70% Analysis Date = 11/03/16 Pct Recovery = 70% Analysis Date = 11/03/16 Pct Recovery = 70% Analysis Date = 10/24/16 Pct Recovery = 70% Analysis Date = 10/24/16 Pct Recovery = 70% Analysis Date = 10/14/16 Pct Recovery = 70% Analysis Date = 10/14/16 Pct Recovery = 70% Analysis Date = 10/04/16 Pct Recovery = 69% Analysis Date = 10/04/16 Pct Recovery = 69% Analysis Date = 09/24/16 Pct Recovery = 69% Analysis Date = 09/24/16 Pct Recovery = 69% Analysis Date = 09/14/16 Pct Recovery = 69% Analysis Date = 09/14/16 Pct Recovery = 69% Analysis Date = 09/04/16 Pct Recovery = 68% Analysis Date = 09/04/16 Pct Recovery = 68% Analysis Date = 08/25/16 Pct Recovery = 68% Analysis Date = 08/25/16 Pct Recovery = 68% Analysis Date = 08/15/16 Pct Recovery = 68% Analysis Date = 08/15/16 Pct Recovery = 68% Analysis Date = 08/05/16 Pct Recovery = 67% Analysis Date = 08/05/16 Pct Recovery = 67% Analysis Date = 07/27/16 Pct Recovery = 67% Analysis Date = 07/27/16 Pct Recovery = 67% Analysis Date = 07/17/16 Pct Recovery = 67% Analysis Date = 07/17/16 Pct Recovery = 67% Analysis Date = 07/07/16 Pct Recovery = 66% Analysis Date = 07/07/16 Pct Recovery = 66% Analysis Date = 06/27/16 Pct Recovery = 66% Analysis Date = 06/27/16 Pct Recovery = 66% Analysis Date = 06/17/16 Pct Recovery = 65% Analysis Date = 06/17/16 Pct Recovery = 65% Analysis Date = 06/07/16 Pct Recovery = 65% Analysis Date = 06/07/16 Pct Recovery = 65% Analysis Date = 05/28/16 Pct Recovery = 65% Analysis Date = 05/28/16 Pct Recovery = 65% Analysis Date = 05/18/16 Pct Recovery = 64% Analysis Date = 05/18/16 Pct Recovery = 64% Analysis Date = 05/08/16 Pct Recovery = 64% Analysis Date = 05/08/16 Pct Recovery = 64% Analysis Date = 04/28/16 Pct Recovery = 63% Analysis Date = 04/28/16 Pct Recovery = 63% Analysis Date = 04/19/16 Pct Recovery = 63% Analysis Date = 04/19/16 Pct Recovery = 63% Analysis Date = 04/09/16 Pct Recovery = 62% Analysis Date = 04/09/16 Pct Recovery = 62% Analysis Date = 03/30/16 Pct Recovery = 62% Analysis Date = 03/30/16 Pct Recovery = 62% Analysis Date = 03/20/16 Pct Recovery = 62% Analysis Date = 03/20/16 Pct Recovery = 62% Analysis Date = 03/10/16 Pct Recovery = 61% Analysis Date = 03/10/16 Pct Recovery = 61% Analysis Date = 02/29/16 Pct Recovery = 61% Analysis Date = 02/29/16 Pct Recovery = 61% Analysis Date = 02/19/16 Pct Recovery = 61% Analysis Date = 02/19/16 Pct Recovery = 61% Analysis Date = 02/09/16 Pct Recovery = 60% Analysis Date = 02/09/16 Pct Recovery = 60% Analysis Date = 01/30/16 Pct Recovery = 60% Analysis Date = 01/30/16 Pct Recovery = 60% Analysis Date = 01/20/16 Pct Recovery = 60% Analysis Date = 01/20/16 Pct Recovery = 60% Analysis Date = 01/11/16 Pct Recovery = 60% Analysis Date = 01/11/16 Pct Recovery = 60% Analysis Date = 01/01/16 Pct Recovery = 60% Analysis Date = 01/01/16 Pct Recovery = 60% Analysis Date = 12/22/15 Pct Recovery = 60% Analysis Date = 12/22/15 Pct Recovery = 60% Analysis Date = 12/12/15 Pct Recovery = 60% Analysis Date = 12/12/15 Pct Recovery = 60% Analysis Date = 12/02/15 Pct Recovery = 60% Analysis Date = 12/02/15 Pct Recovery = 60% Analysis Date = 11/22/15 Pct Recovery = 60% Analysis Date = 11/22/15 Pct Recovery = 60% Analysis Date = 11/12/15 Pct Recovery = 60% Analysis Date = 11/12/15 Pct Recovery = 60% Analysis Date = 11/02/15 Pct Recovery = 60% Analysis Date = 11/02/15 Pct Recovery = 60% Analysis Date = 10/23/15 Pct Recovery = 60% Analysis Date = 10/23/15 Pct Recovery = 60% Analysis Date = 10/13/15 Pct Recovery = 60% Analysis Date = 10/13/15 Pct Recovery = 60% Analysis Date = 10/04/15 Pct Recovery = 60% Analysis Date = 10/04/15 Pct Recovery = 60% Analysis Date = 09/24/15 Pct Recovery = 60% Analysis Date = 09/24/15 Pct Recovery = 60% Analysis Date = 09/14/15 Pct Recovery = 60% Analysis Date = 09/14/15 Pct Recovery = 60% Analysis Date = 09/04/15 Pct Recovery = 60% Analysis Date = 09/04/15 Pct Recovery = 60% Analysis Date = 08/25/15 Pct Recovery = 60% Analysis Date = 08/25/15 Pct Recovery = 60% Analysis Date = 08/15/15 Pct Recovery = 60% Analysis Date = 08/15/15 Pct Recovery = 60% Analysis Date = 08/05/15 Pct Recovery = 59% Analysis Date = 08/05/15 Pct Recovery = 59% Analysis Date = 07/26/15 Pct Recovery = 59% Analysis Date = 07/26/15 Pct Recovery = 59% Analysis Date = 07/16/15 Pct Recovery = 59% Analysis Date = 07/16/15 Pct Recovery = 59% Analysis Date = 07/06/15 Pct Recovery = 59% Analysis Date = 07/06/15 Pct Recovery = 59% Analysis Date = 06/27/15 Pct Recovery = 59% Analysis Date = 06/27/15 Pct Recovery = 59% Analysis Date = 06/17/15 Pct Recovery = 59% Analysis Date = 06/17/15 Pct Recovery = 59% Analysis Date = 06/07/15 Pct Recovery = 59% Analysis Date = 06/07/15 Pct Recovery = 59% Analysis Date = 05/28/15 Pct Recovery = 59% Analysis Date = 05/28/15 Pct Recovery = 59% Analysis Date = 05/18/15 Pct Recovery = 59% Analysis Date = 05/18/15 Pct Recovery = 59% Analysis Date = 05/08/15 Pct Recovery = 59% Analysis Date = 05/08/15 Pct Recovery = 59% Analysis Date = 04/28/15 Pct Recovery = 59% Analysis Date = 04/28/15 Pct Recovery = 59% Analysis Date = 04/18/15 Pct Recovery = 59% Analysis Date = 04/18/15 Pct Recovery = 59% Analysis Date = 04/08/15 Pct Recovery = 59% Analysis Date = 04/08/15 Pct Recovery = 59% Analysis Date = 03/29/15 Pct Recovery = 59% Analysis Date = 03/29/15 Pct Recovery = 59% Analysis Date = 03/20/15 Pct Recovery = 59% Analysis Date = 03/20/15 Pct Recovery = 59% Analysis Date = 03/10/15 Pct Recovery = 59% Analysis Date = 03/10/15 Pct Recovery = 59% Analysis Date = 02/28/15 Pct Recovery = 59% Analysis Date = 02/28/15 Pct Recovery = 59% Analysis Date = 02/18/15 Pct Recovery = 59% Analysis Date = 02/18/15 Pct Recovery = 59% Analysis Date = 02/08/15 Pct Recovery = 59% Analysis Date = 02/08/15 Pct Recovery = 59% Analysis Date = 01/29/15 Pct Recovery = 59% Analysis Date = 01/29/15 Pct Recovery = 59% Analysis Date = 01/19/15 Pct Recovery = 59% Analysis Date = 01/19/15 Pct Recovery = 59% Analysis Date = 01/09/15 Pct Recovery = 59% Analysis Date = 01/09/15 Pct Recovery = 59% Analysis Date = 12/30/14 Pct Recovery = 59% Analysis Date = 12/30/14 Pct Recovery = 59% Analysis Date = 12/20/14 Pct Recovery = 59% Analysis Date = 12/20/14 Pct Recovery = 59% Analysis Date = 12/11/14 Pct Recovery = 59% Analysis Date = 12/11/14 Pct Recovery = 59% Analysis Date = 12/01/14 Pct Recovery = 59% Analysis Date = 12/01/14 Pct Recovery = 59% Analysis Date = 11/21/14 Pct Recovery = 59% Analysis Date = 11/21/14 Pct Recovery = 59% Analysis Date = 11/11/14 Pct Recovery = 59% Analysis Date = 11/11/14 Pct Recovery = 59% Analysis Date = 11/01/14 Pct Recovery = 59% Analysis Date = 11/01/14 Pct Recovery = 59% Analysis Date = 10/22/14 Pct Recovery = 59% Analysis Date = 10/22/14 Pct Recovery = 59% Analysis Date = 10/12/14 Pct Recovery = 59% Analysis Date = 10/12/14 Pct Recovery = 59% Analysis Date = 10/02/14 Pct Recovery = 59% Analysis Date = 10/02/14 Pct Recovery = 59% Analysis Date = 09/22/14 Pct Recovery = 59% Analysis Date = 09/22/14 Pct Recovery = 59% Analysis Date = 09/12/14 Pct Recovery = 59% Analysis Date = 09/12/14 Pct Recovery = 59% Analysis Date = 09/03/14 Pct Recovery = 59% Analysis Date = 09/03/14 Pct Recovery = 59% Analysis Date = 08/24/14 Pct Recovery = 58% Analysis Date = 08/24/14 Pct Recovery = 58% Analysis Date = 08/14/14 Pct Recovery = 58% Analysis Date = 08/14/14 Pct Recovery = 58% Analysis Date = 08/04/14 Pct Recovery = 58% Analysis Date = 08/04/14 Pct Recovery = 58% Analysis Date = 07/25/14 Pct Recovery = 58% Analysis Date = 07/25/14 Pct Recovery = 58% Analysis Date = 07/15/14 Pct Recovery = 58% Analysis Date = 07/15/14 Pct Recovery = 58% Analysis Date = 07/05/14 Pct Recovery = 59% Analysis Date = 07/05/14 Pct Recovery = 59% Analysis Date = 06/25/14 Pct Recovery = 59% Analysis Date = 06/25/14 Pct Recovery = 59% Analysis Date = 06/15/14 Pct Recovery = 59% Analysis Date = 06/15/14 Pct Recovery = 59% Analysis Date = 06/05/14 Pct Recovery = 59% Analysis Date = 06/05/14 Pct Recovery = 59% Analysis Date = 05/27/14 Pct Recovery = 59% Analysis Date = 05/27/14 Pct Recovery = 59% Analysis Date = 05/17/14 Pct Recovery = 59% Analysis Date = 05/17/14 Pct Recovery = 59% Analysis Date = 05/07/14 Pct Recovery = 59% Analysis Date = 05/07/14 Pct Recovery = 59% Analysis Date = 04/27/14 Pct Recovery = 59% Analysis Date = 04/27/14 Pct Recovery = 59% Analysis Date = 04/17/14 Pct Recovery = 59% Analysis Date = 04/17/14 Pct Recovery = 59% Analysis Date = 04/07/14 Pct Recovery = 59% Analysis Date = 04/07/14 Pct Recovery = 59% Analysis Date = 03/28/14 Pct Recovery = 59% Analysis Date = 03/28/14 Pct Recovery = 59% Analysis Date = 03/18/14 Pct Recovery = 59% Analysis Date = 03/18/14 Pct Recovery = 59% Analysis Date = 03/08/14 Pct Recovery = 59% Analysis Date = 03/08/14 Pct Recovery = 59% Analysis Date = 02/26/14 Pct Recovery = 59% Analysis Date = 02/26/14 Pct Recovery = 59% Analysis Date = 02/17/14 Pct Recovery = 59% Analysis Date = 02/17/14 Pct Recovery = 59% Analysis Date = 02/07/14 Pct Recovery = 59% Analysis Date = 02/07/14 Pct Recovery = 59% Analysis Date = 01/28/14 Pct Recovery = 59% Analysis Date = 01/28/14 Pct Recovery = 59% Analysis Date = 01/18/14 Pct Recovery = 58% Analysis Date = 01/18/14 Pct Recovery = 58% Analysis Date = 01/08/14 Pct Recovery = 58% Analysis Date = 01/08/14 Pct Recovery = 58% Analysis Date = 12/29/13 Pct Recovery = 58% Analysis Date = 12/29/13 Pct Recovery = 58% Analysis Date = 12/19/13 Pct Recovery = 58% Analysis Date = 12/19/13 Pct Recovery = 58% Analysis Date = 12/09/13 Pct Recovery = 58% Analysis Date = 12/09/13 Pct Recovery = 58% Analysis Date = 11/29/13 Pct Recovery = 58% Analysis Date = 11/29/13 Pct Recovery = 58% Analysis Date = 11/19/13 Pct Recovery = 58% Analysis Date = 11/19/13 Pct Recovery = 58% Analysis Date = 11/10/13 Pct Recovery = 57% Analysis Date = 11/10/13 Pct Recovery = 57% Analysis Date = 10/31/13 Pct Recovery = 57% Analysis Date = 10/31/13 Pct Recovery = 57% Analysis Date = 10/21/13 Pct Recovery = 57% Analysis Date = 10/21/13 Pct Recovery = 57% Analysis Date = 10/11/13 Pct Recovery = 57% Analysis Date = 10/11/13 Pct Recovery = 57% Analysis Date = 10/01/13 Pct Recovery = 57% Analysis Date = 10/01/13 Pct Recovery = 57% Analysis Date = 09/21/13 Pct Recovery = 57% Analysis Date = 09/21/13 Pct Recovery = 57% Analysis Date = 09/11/13 Pct Recovery = 56% Analysis Date = 09/11/13 Pct Recovery = 56% Analysis Date = 09/01/13 Pct Recovery = 56% Analysis Date = 09/01/13 Pct Recovery = 56% Analysis Date = 08/22/13 Pct Recovery = 56% Analysis Date = 08/22/13 Pct Recovery = 56% Analysis Date = 08/12/13 Pct Recovery = 56% Analysis Date = 08/12/13 Pct Recovery = 56% Analysis Date = 08/03/13 Pct Recovery = 56% Analysis Date = 08/03/13 Pct Recovery = 56% Analysis Date = 07/24/13 Pct Recovery = 56% Analysis Date = 07/24/13 Pct Recovery = 56% Analysis Date = 07/14/13 Pct Recovery = 55% Analysis Date = 07/14/13 Pct Recovery = 55% Analysis Date = 07/04/13 Pct Recovery = 55% Analysis Date = 07/04/13 Pct Recovery = 55% Analysis Date = 06/24/13 Pct Recovery = 55% Analysis Date = 06/24/13 Pct Recovery = 55% Analysis Date = 06/14/13 Pct Recovery = 55% Analysis Date = 06/14/13 Pct Recovery = 55% Analysis Date = 06/04/13 Pct Recovery = 55% Analysis Date = 06/04/13 Pct Recovery = 55% Analysis Date = 05/25/13 Pct Recovery = 54% Analysis Date = 05/25/13 Pct Recovery = 54% Analysis Date = 05/15/13 Pct Recovery = 54% Analysis Date = 05/15/13 Pct Recovery = 54% Analysis Date = 05/05/13 Pct Recovery = 54% Analysis Date = 05/05/13 Pct Recovery = 54% Analysis Date = 04/26/13 Pct Recovery = 54% Analysis Date = 04/26/13 Pct Recovery = 54% Analysis Date = 04/16/13 Pct Recovery = 54% Analysis Date = 04/16/13 Pct Recovery = 54% Analysis Date = 04/06/13 Pct Recovery = 53% Analysis Date = 04/06/13 Pct Recovery = 53% Analysis Date = 03/27/13 Pct Recovery = 53% Analysis Date = 03/27/13 Pct Recovery = 53% Analysis Date = 03/17/13 Pct Recovery = 53% Analysis Date = 03/17/13 Pct Recovery = 53% Analysis Date = 03/07/13 Pct Recovery = 53% Analysis Date = 03/07/13 Pct Recovery = 53% Analysis Date = 02/25/13 Pct Recovery = 52% Analysis Date = 02/25/13 Pct Recovery = 52% Analysis Date = 02/15/13 Pct Recovery = 52% Analysis Date = 02/15/13 Pct Recovery = 52% Analysis Date = 02/05/13 Pct Recovery = 52% Analysis Date = 02/05/13 Pct Recovery = 52% Analysis Date = 01/26/13 Pct Recovery = 52% Analysis Date = 01/26/13 Pct Recovery = 52% Analysis Date = 01/17/13 Pct Recovery = 52% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
PHORATE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 63 65% 21% 69% 21%
Total 63 65% 21% 69% 21%

Sample Statistics
PHORATE

Characteristic N % % Basis
Plotted 63 86% Spiked
Estimated Values 0 0% Spiked
Deleted Values 1 1% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 73 .  
False Negatives 10 14% 10 out of 73
Not Spiked 53 .  
False Positives 0 0% 0 out of 52

OBSP Determination:
PHORATE OXON
METHOD: 2033 , TESTIDCODE: 61666GCM39

Laboratory ID = 20140100085 Lab Value = 0.293 Expected Conc. = 0.376 Report level label = 0.027 Pct Recovery = 78% Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl SpecificMix = 042413 Laboratory ID = 20130250061 Lab Value = 0.101 Expected Conc. = 0.198 Report level label = 0.027 Pct Recovery = 51% Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl SpecificMix = 05BB029 Laboratory ID = 20132140002 Lab Value = 0.037 Expected Conc. = 0.189 Report level label = 0.027 Pct Recovery = 20% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl SpecificMix = 04CC101 Laboratory ID = 20132690010 Lab Value = 0.126 Expected Conc. = 0.188 Report level label = 0.027 Pct Recovery = 67% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl SpecificMix = 042413 Laboratory ID = 20132560001 Lab Value = 0.086 Expected Conc. = 0.188 Report level label = 0.027 Pct Recovery = 46% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl SpecificMix = 042413 Laboratory ID = 20172510330 Lab Value = 0.114 Expected Conc. = 0.18 Report level label = 0.027 Pct Recovery = 63% Analysis Date = 12/29/17 SpikeMix = ChemService 6537100: 100 µl & Abs 071817Pest: 100 µl SpecificMix = 071817Pest Laboratory ID = 20161880109 Lab Value = 0.158 Expected Conc. = 0.167 Report level label = 0.027 Pct Recovery = 95% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl SpecificMix = 03FF076 Laboratory ID = 20170960001 Lab Value = 0.092 Expected Conc. = 0.1336 Report level label = 0.027 Pct Recovery = 69% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl SpecificMix = 03FF076 Laboratory ID = 20150720069 Lab Value = 0.053 Expected Conc. = 0.1068 Report level label = 0.027 Pct Recovery = 50% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 0227-14-08 Laboratory ID = 20141770149 Lab Value = 0.062 Expected Conc. = 0.1068 Report level label = 0.027 Pct Recovery = 58% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl SpecificMix = 0227-14-08 Laboratory ID = 20141570088 Lab Value = 0.084 Expected Conc. = 0.1068 Report level label = 0.027 Pct Recovery = 78% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl SpecificMix = 0227-14-08 Laboratory ID = 20140230082 Lab Value = 0.057 Expected Conc. = 0.1 Report level label = 0.027 Pct Recovery = 57% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl SpecificMix = 012513 Laboratory ID = 20132420001 Lab Value = 0.049 Expected Conc. = 0.1 Report level label = 0.027 Pct Recovery = 49% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl SpecificMix = 012513 Laboratory ID = 20130940097 Lab Value = 0.035 Expected Conc. = 0.1 Report level label = 0.027 Pct Recovery = 35% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = 052412 Laboratory ID = 20130100066 Lab Value = 0.070 Expected Conc. = 0.1 Report level label = 0.027 Pct Recovery = 70% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl SpecificMix = 052412 Laboratory ID = 20172560101 Lab Value = 0.060 Expected Conc. = 0.09 Report level label = 0.027 Pct Recovery = 66% Analysis Date = 12/22/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6567600: 50 µl SpecificMix = 6567600 Laboratory ID = 20161260151 Lab Value = 0.051 Expected Conc. = 0.0812 Report level label = 0.027 Pct Recovery = 63% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = EN150513008 Laboratory ID = 20160770090 Lab Value = 0.044 Expected Conc. = 0.0812 Report level label = 0.027 Pct Recovery = 55% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = EN150513008 Laboratory ID = 20153510109 Lab Value = 0.037 Expected Conc. = 0.0812 Report level label = 0.027 Pct Recovery = 46% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = EN150513008 Laboratory ID = 20140730138 Lab Value = 0.041 Expected Conc. = 0.0756 Report level label = 0.027 Pct Recovery = 54% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 04CC101 Laboratory ID = 20140510043 Lab Value = 0.032 Expected Conc. = 0.0756 Report level label = 0.027 Pct Recovery = 42% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 04CC101 Laboratory ID = 20133310030 Lab Value = 0.061 Expected Conc. = 0.0756 Report level label = 0.027 Pct Recovery = 81% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl SpecificMix = 04CC101 Laboratory ID = 20132280016 Lab Value = 0.030 Expected Conc. = 0.0756 Report level label = 0.027 Pct Recovery = 40% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl SpecificMix = 04CC101 Laboratory ID = 20133580036 Lab Value = 0.033 Expected Conc. = 0.0752 Report level label = 0.027 Pct Recovery = 43% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 042413 Laboratory ID = 20133190012 Lab Value = 0.053 Expected Conc. = 0.0752 Report level label = 0.027 Pct Recovery = 70% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 042413 Laboratory ID = 20131650073 Lab Value = 0.016 Expected Conc. = 0.0752 Report level label = 0.027 Pct Recovery = 22% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl SpecificMix = 042413 Laboratory ID = 20172020035 Lab Value = 0.055 Expected Conc. = 0.0668 Report level label = 0.027 Pct Recovery = 82% Analysis Date = 11/07/17 SpikeMix = Abs 071717Pest: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20171510080 Lab Value = 0.058 Expected Conc. = 0.0668 Report level label = 0.027 Pct Recovery = 87% Analysis Date = 06/09/17 SpikeMix = Supelco LC20138V: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20170460061 Lab Value = 0.046 Expected Conc. = 0.0668 Report level label = 0.027 Pct Recovery = 69% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl SpecificMix = 03FF076 Laboratory ID = 20162660005 Lab Value = 0.045 Expected Conc. = 0.0668 Report level label = 0.027 Pct Recovery = 67% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl SpecificMix = 03FF076 Laboratory ID = 20161600087 Lab Value = 0.061 Expected Conc. = 0.0668 Report level label = 0.027 Pct Recovery = 92% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20161340228 Lab Value = 0.049 Expected Conc. = 0.0668 Report level label = 0.027 Pct Recovery = 73% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl SpecificMix = 03FF076 Laboratory ID = 20161190075 Lab Value = 0.045 Expected Conc. = 0.0668 Report level label = 0.027 Pct Recovery = 68% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20172780018 Lab Value = 0.031 Expected Conc. = 0.054 Report level label = 0.027 Pct Recovery = 57% Analysis Date = 02/08/18 SpikeMix = ChemService 6537100: 30 µl & Abs 071817Pest: 30 µl SpecificMix = 071817Pest Laboratory ID = 20141840097 Lab Value = 0.027 Expected Conc. = 0.0534 Report level label = 0.027 Pct Recovery = 50% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20141490205 Lab Value = 0.051 Expected Conc. = 0.0534 Report level label = 0.027 Pct Recovery = 95% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20141420140 Lab Value = 0.039 Expected Conc. = 0.0534 Report level label = 0.027 Pct Recovery = 73% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20141360094 Lab Value = 0.030 Expected Conc. = 0.0534 Report level label = 0.027 Pct Recovery = 56% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20160560044 Lab Value = 0.026 Expected Conc. = 0.0406 Report level label = 0.027 Pct Recovery = 65% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl SpecificMix = EN150513008 Laboratory ID = 20153160001 Lab Value = 0.014 Expected Conc. = 0.0406 Report level label = 0.027 Pct Recovery = 33% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = EN150513008 Laboratory ID = 20153030068 Lab Value = 0.025 Expected Conc. = 0.0406 Report level label = 0.027 Pct Recovery = 61% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150513008 Laboratory ID = 20151480170 Lab Value = 0.003 Expected Conc. = 0.0406 Report level label = 0.027 Pct Recovery = 8% Analysis Date = 06/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150513008 Laboratory ID = 20161050143 Lab Value = 0.034 Expected Conc. = 0.0404 Report level label = 0.027 Pct Recovery = 83% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Laboratory ID = 20160430111 Lab Value = 0.044 Expected Conc. = 0.0404 Report level label = 0.027 Pct Recovery = 108% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Laboratory ID = 20160070059 Lab Value = 0.025 Expected Conc. = 0.0404 Report level label = 0.027 Pct Recovery = 62% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = 040615 Laboratory ID = 20151380009 Lab Value = 0.023 Expected Conc. = 0.0404 Report level label = 0.027 Pct Recovery = 57% Analysis Date = 05/30/15 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Laboratory ID = 20151210037 Lab Value = 0.028 Expected Conc. = 0.0404 Report level label = 0.027 Pct Recovery = 68% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Laboratory ID = 20140860102 Lab Value = 0.022 Expected Conc. = 0.04 Report level label = 0.027 Pct Recovery = 55% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 012513 Laboratory ID = 20133400002 Lab Value = 0.028 Expected Conc. = 0.04 Report level label = 0.027 Pct Recovery = 69% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = 052412 Laboratory ID = 20132910008 Lab Value = 0.025 Expected Conc. = 0.04 Report level label = 0.027 Pct Recovery = 63% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = 052412 Laboratory ID = 20131920149 Lab Value = 0.017 Expected Conc. = 0.04 Report level label = 0.027 Pct Recovery = 43% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl SpecificMix = 012513 Laboratory ID = 20130650005 Lab Value = 0.024 Expected Conc. = 0.04 Report level label = 0.027 Pct Recovery = 61% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl SpecificMix = 052412 Laboratory ID = 20130510051 Lab Value = 0.019 Expected Conc. = 0.0396 Report level label = 0.027 Pct Recovery = 47% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl SpecificMix = 05BB029 Analysis Date = 02/08/18 Pct Recovery = 74% Analysis Date = 01/29/18 Pct Recovery = 74% Analysis Date = 01/29/18 Pct Recovery = 74% Analysis Date = 01/20/18 Pct Recovery = 74% Analysis Date = 01/20/18 Pct Recovery = 74% Analysis Date = 01/11/18 Pct Recovery = 74% Analysis Date = 01/11/18 Pct Recovery = 74% Analysis Date = 01/02/18 Pct Recovery = 74% Analysis Date = 01/02/18 Pct Recovery = 74% Analysis Date = 12/23/17 Pct Recovery = 74% Analysis Date = 12/23/17 Pct Recovery = 74% Analysis Date = 12/14/17 Pct Recovery = 74% Analysis Date = 12/14/17 Pct Recovery = 74% Analysis Date = 12/05/17 Pct Recovery = 74% Analysis Date = 12/05/17 Pct Recovery = 74% Analysis Date = 11/26/17 Pct Recovery = 74% Analysis Date = 11/26/17 Pct Recovery = 74% Analysis Date = 11/16/17 Pct Recovery = 74% Analysis Date = 11/16/17 Pct Recovery = 74% Analysis Date = 11/07/17 Pct Recovery = 73% Analysis Date = 11/07/17 Pct Recovery = 73% Analysis Date = 10/29/17 Pct Recovery = 73% Analysis Date = 10/29/17 Pct Recovery = 73% Analysis Date = 10/20/17 Pct Recovery = 73% Analysis Date = 10/20/17 Pct Recovery = 73% Analysis Date = 10/10/17 Pct Recovery = 73% Analysis Date = 10/10/17 Pct Recovery = 73% Analysis Date = 10/01/17 Pct Recovery = 73% Analysis Date = 10/01/17 Pct Recovery = 73% Analysis Date = 09/22/17 Pct Recovery = 73% Analysis Date = 09/22/17 Pct Recovery = 73% Analysis Date = 09/13/17 Pct Recovery = 73% Analysis Date = 09/13/17 Pct Recovery = 73% Analysis Date = 09/03/17 Pct Recovery = 73% Analysis Date = 09/03/17 Pct Recovery = 73% Analysis Date = 08/25/17 Pct Recovery = 73% Analysis Date = 08/25/17 Pct Recovery = 73% Analysis Date = 08/16/17 Pct Recovery = 73% Analysis Date = 08/16/17 Pct Recovery = 73% Analysis Date = 08/07/17 Pct Recovery = 73% Analysis Date = 08/07/17 Pct Recovery = 73% Analysis Date = 07/28/17 Pct Recovery = 73% Analysis Date = 07/28/17 Pct Recovery = 73% Analysis Date = 07/19/17 Pct Recovery = 72% Analysis Date = 07/19/17 Pct Recovery = 72% Analysis Date = 07/10/17 Pct Recovery = 72% Analysis Date = 07/10/17 Pct Recovery = 72% Analysis Date = 07/01/17 Pct Recovery = 72% Analysis Date = 07/01/17 Pct Recovery = 72% Analysis Date = 06/22/17 Pct Recovery = 72% Analysis Date = 06/22/17 Pct Recovery = 72% Analysis Date = 06/12/17 Pct Recovery = 72% Analysis Date = 06/12/17 Pct Recovery = 72% Analysis Date = 06/03/17 Pct Recovery = 72% Analysis Date = 06/03/17 Pct Recovery = 72% Analysis Date = 05/25/17 Pct Recovery = 72% Analysis Date = 05/25/17 Pct Recovery = 72% Analysis Date = 05/16/17 Pct Recovery = 72% Analysis Date = 05/16/17 Pct Recovery = 72% Analysis Date = 05/06/17 Pct Recovery = 72% Analysis Date = 05/06/17 Pct Recovery = 72% Analysis Date = 04/27/17 Pct Recovery = 72% Analysis Date = 04/27/17 Pct Recovery = 72% Analysis Date = 04/18/17 Pct Recovery = 72% Analysis Date = 04/18/17 Pct Recovery = 72% Analysis Date = 04/09/17 Pct Recovery = 72% Analysis Date = 04/09/17 Pct Recovery = 72% Analysis Date = 03/30/17 Pct Recovery = 71% Analysis Date = 03/30/17 Pct Recovery = 71% Analysis Date = 03/21/17 Pct Recovery = 71% Analysis Date = 03/21/17 Pct Recovery = 71% Analysis Date = 03/12/17 Pct Recovery = 71% Analysis Date = 03/12/17 Pct Recovery = 71% Analysis Date = 03/03/17 Pct Recovery = 71% Analysis Date = 03/03/17 Pct Recovery = 71% Analysis Date = 02/21/17 Pct Recovery = 71% Analysis Date = 02/21/17 Pct Recovery = 71% Analysis Date = 02/12/17 Pct Recovery = 71% Analysis Date = 02/12/17 Pct Recovery = 71% Analysis Date = 02/03/17 Pct Recovery = 71% Analysis Date = 02/03/17 Pct Recovery = 71% Analysis Date = 01/25/17 Pct Recovery = 71% Analysis Date = 01/25/17 Pct Recovery = 71% Analysis Date = 01/15/17 Pct Recovery = 70% Analysis Date = 01/15/17 Pct Recovery = 70% Analysis Date = 01/06/17 Pct Recovery = 70% Analysis Date = 01/06/17 Pct Recovery = 70% Analysis Date = 12/28/16 Pct Recovery = 70% Analysis Date = 12/28/16 Pct Recovery = 70% Analysis Date = 12/19/16 Pct Recovery = 70% Analysis Date = 12/19/16 Pct Recovery = 70% Analysis Date = 12/09/16 Pct Recovery = 70% Analysis Date = 12/09/16 Pct Recovery = 70% Analysis Date = 11/30/16 Pct Recovery = 70% Analysis Date = 11/30/16 Pct Recovery = 70% Analysis Date = 11/21/16 Pct Recovery = 70% Analysis Date = 11/21/16 Pct Recovery = 70% Analysis Date = 11/12/16 Pct Recovery = 70% Analysis Date = 11/12/16 Pct Recovery = 70% Analysis Date = 11/03/16 Pct Recovery = 69% Analysis Date = 11/03/16 Pct Recovery = 69% Analysis Date = 10/24/16 Pct Recovery = 69% Analysis Date = 10/24/16 Pct Recovery = 69% Analysis Date = 10/15/16 Pct Recovery = 69% Analysis Date = 10/15/16 Pct Recovery = 69% Analysis Date = 10/06/16 Pct Recovery = 69% Analysis Date = 10/06/16 Pct Recovery = 69% Analysis Date = 09/27/16 Pct Recovery = 69% Analysis Date = 09/27/16 Pct Recovery = 69% Analysis Date = 09/17/16 Pct Recovery = 69% Analysis Date = 09/17/16 Pct Recovery = 69% Analysis Date = 09/08/16 Pct Recovery = 69% Analysis Date = 09/08/16 Pct Recovery = 69% Analysis Date = 08/30/16 Pct Recovery = 69% Analysis Date = 08/30/16 Pct Recovery = 69% Analysis Date = 08/21/16 Pct Recovery = 68% Analysis Date = 08/21/16 Pct Recovery = 68% Analysis Date = 08/11/16 Pct Recovery = 68% Analysis Date = 08/11/16 Pct Recovery = 68% Analysis Date = 08/02/16 Pct Recovery = 68% Analysis Date = 08/02/16 Pct Recovery = 68% Analysis Date = 07/24/16 Pct Recovery = 68% Analysis Date = 07/24/16 Pct Recovery = 68% Analysis Date = 07/15/16 Pct Recovery = 68% Analysis Date = 07/15/16 Pct Recovery = 68% Analysis Date = 07/05/16 Pct Recovery = 68% Analysis Date = 07/05/16 Pct Recovery = 68% Analysis Date = 06/26/16 Pct Recovery = 67% Analysis Date = 06/26/16 Pct Recovery = 67% Analysis Date = 06/17/16 Pct Recovery = 67% Analysis Date = 06/17/16 Pct Recovery = 67% Analysis Date = 06/08/16 Pct Recovery = 67% Analysis Date = 06/08/16 Pct Recovery = 67% Analysis Date = 05/29/16 Pct Recovery = 67% Analysis Date = 05/29/16 Pct Recovery = 67% Analysis Date = 05/20/16 Pct Recovery = 67% Analysis Date = 05/20/16 Pct Recovery = 67% Analysis Date = 05/11/16 Pct Recovery = 67% Analysis Date = 05/11/16 Pct Recovery = 67% Analysis Date = 05/02/16 Pct Recovery = 66% Analysis Date = 05/02/16 Pct Recovery = 66% Analysis Date = 04/22/16 Pct Recovery = 66% Analysis Date = 04/22/16 Pct Recovery = 66% Analysis Date = 04/13/16 Pct Recovery = 66% Analysis Date = 04/13/16 Pct Recovery = 66% Analysis Date = 04/04/16 Pct Recovery = 65% Analysis Date = 04/04/16 Pct Recovery = 65% Analysis Date = 03/26/16 Pct Recovery = 65% Analysis Date = 03/26/16 Pct Recovery = 65% Analysis Date = 03/17/16 Pct Recovery = 65% Analysis Date = 03/17/16 Pct Recovery = 65% Analysis Date = 03/07/16 Pct Recovery = 64% Analysis Date = 03/07/16 Pct Recovery = 64% Analysis Date = 02/27/16 Pct Recovery = 64% Analysis Date = 02/27/16 Pct Recovery = 64% Analysis Date = 02/18/16 Pct Recovery = 64% Analysis Date = 02/18/16 Pct Recovery = 64% Analysis Date = 02/09/16 Pct Recovery = 63% Analysis Date = 02/09/16 Pct Recovery = 63% Analysis Date = 01/30/16 Pct Recovery = 63% Analysis Date = 01/30/16 Pct Recovery = 63% Analysis Date = 01/21/16 Pct Recovery = 63% Analysis Date = 01/21/16 Pct Recovery = 63% Analysis Date = 01/12/16 Pct Recovery = 63% Analysis Date = 01/12/16 Pct Recovery = 63% Analysis Date = 01/03/16 Pct Recovery = 63% Analysis Date = 01/03/16 Pct Recovery = 63% Analysis Date = 12/24/15 Pct Recovery = 62% Analysis Date = 12/24/15 Pct Recovery = 62% Analysis Date = 12/15/15 Pct Recovery = 62% Analysis Date = 12/15/15 Pct Recovery = 62% Analysis Date = 12/06/15 Pct Recovery = 62% Analysis Date = 12/06/15 Pct Recovery = 62% Analysis Date = 11/27/15 Pct Recovery = 62% Analysis Date = 11/27/15 Pct Recovery = 62% Analysis Date = 11/17/15 Pct Recovery = 62% Analysis Date = 11/17/15 Pct Recovery = 62% Analysis Date = 11/08/15 Pct Recovery = 62% Analysis Date = 11/08/15 Pct Recovery = 62% Analysis Date = 10/30/15 Pct Recovery = 61% Analysis Date = 10/30/15 Pct Recovery = 61% Analysis Date = 10/21/15 Pct Recovery = 61% Analysis Date = 10/21/15 Pct Recovery = 61% Analysis Date = 10/11/15 Pct Recovery = 61% Analysis Date = 10/11/15 Pct Recovery = 61% Analysis Date = 10/02/15 Pct Recovery = 61% Analysis Date = 10/02/15 Pct Recovery = 61% Analysis Date = 09/23/15 Pct Recovery = 61% Analysis Date = 09/23/15 Pct Recovery = 61% Analysis Date = 09/14/15 Pct Recovery = 60% Analysis Date = 09/14/15 Pct Recovery = 60% Analysis Date = 09/04/15 Pct Recovery = 60% Analysis Date = 09/04/15 Pct Recovery = 60% Analysis Date = 08/26/15 Pct Recovery = 60% Analysis Date = 08/26/15 Pct Recovery = 60% Analysis Date = 08/17/15 Pct Recovery = 60% Analysis Date = 08/17/15 Pct Recovery = 60% Analysis Date = 08/08/15 Pct Recovery = 60% Analysis Date = 08/08/15 Pct Recovery = 60% Analysis Date = 07/30/15 Pct Recovery = 59% Analysis Date = 07/30/15 Pct Recovery = 59% Analysis Date = 07/20/15 Pct Recovery = 59% Analysis Date = 07/20/15 Pct Recovery = 59% Analysis Date = 07/11/15 Pct Recovery = 59% Analysis Date = 07/11/15 Pct Recovery = 59% Analysis Date = 07/02/15 Pct Recovery = 59% Analysis Date = 07/02/15 Pct Recovery = 59% Analysis Date = 06/23/15 Pct Recovery = 59% Analysis Date = 06/23/15 Pct Recovery = 59% Analysis Date = 06/13/15 Pct Recovery = 59% Analysis Date = 06/13/15 Pct Recovery = 59% Analysis Date = 06/04/15 Pct Recovery = 58% Analysis Date = 06/04/15 Pct Recovery = 58% Analysis Date = 05/26/15 Pct Recovery = 58% Analysis Date = 05/26/15 Pct Recovery = 58% Analysis Date = 05/17/15 Pct Recovery = 58% Analysis Date = 05/17/15 Pct Recovery = 58% Analysis Date = 05/07/15 Pct Recovery = 58% Analysis Date = 05/07/15 Pct Recovery = 58% Analysis Date = 04/28/15 Pct Recovery = 58% Analysis Date = 04/28/15 Pct Recovery = 58% Analysis Date = 04/19/15 Pct Recovery = 58% Analysis Date = 04/19/15 Pct Recovery = 58% Analysis Date = 04/10/15 Pct Recovery = 58% Analysis Date = 04/10/15 Pct Recovery = 58% Analysis Date = 03/31/15 Pct Recovery = 58% Analysis Date = 03/31/15 Pct Recovery = 58% Analysis Date = 03/22/15 Pct Recovery = 59% Analysis Date = 03/22/15 Pct Recovery = 59% Analysis Date = 03/13/15 Pct Recovery = 59% Analysis Date = 03/13/15 Pct Recovery = 59% Analysis Date = 03/04/15 Pct Recovery = 59% Analysis Date = 03/04/15 Pct Recovery = 59% Analysis Date = 02/22/15 Pct Recovery = 59% Analysis Date = 02/22/15 Pct Recovery = 59% Analysis Date = 02/13/15 Pct Recovery = 59% Analysis Date = 02/13/15 Pct Recovery = 59% Analysis Date = 02/04/15 Pct Recovery = 59% Analysis Date = 02/04/15 Pct Recovery = 59% Analysis Date = 01/26/15 Pct Recovery = 59% Analysis Date = 01/26/15 Pct Recovery = 59% Analysis Date = 01/16/15 Pct Recovery = 59% Analysis Date = 01/16/15 Pct Recovery = 59% Analysis Date = 01/07/15 Pct Recovery = 59% Analysis Date = 01/07/15 Pct Recovery = 59% Analysis Date = 12/29/14 Pct Recovery = 59% Analysis Date = 12/29/14 Pct Recovery = 59% Analysis Date = 12/20/14 Pct Recovery = 59% Analysis Date = 12/20/14 Pct Recovery = 59% Analysis Date = 12/11/14 Pct Recovery = 59% Analysis Date = 12/11/14 Pct Recovery = 59% Analysis Date = 12/01/14 Pct Recovery = 59% Analysis Date = 12/01/14 Pct Recovery = 59% Analysis Date = 11/22/14 Pct Recovery = 59% Analysis Date = 11/22/14 Pct Recovery = 59% Analysis Date = 11/13/14 Pct Recovery = 59% Analysis Date = 11/13/14 Pct Recovery = 59% Analysis Date = 11/04/14 Pct Recovery = 59% Analysis Date = 11/04/14 Pct Recovery = 59% Analysis Date = 10/25/14 Pct Recovery = 59% Analysis Date = 10/25/14 Pct Recovery = 59% Analysis Date = 10/16/14 Pct Recovery = 59% Analysis Date = 10/16/14 Pct Recovery = 59% Analysis Date = 10/07/14 Pct Recovery = 59% Analysis Date = 10/07/14 Pct Recovery = 59% Analysis Date = 09/28/14 Pct Recovery = 59% Analysis Date = 09/28/14 Pct Recovery = 59% Analysis Date = 09/18/14 Pct Recovery = 59% Analysis Date = 09/18/14 Pct Recovery = 59% Analysis Date = 09/09/14 Pct Recovery = 59% Analysis Date = 09/09/14 Pct Recovery = 59% Analysis Date = 08/31/14 Pct Recovery = 59% Analysis Date = 08/31/14 Pct Recovery = 59% Analysis Date = 08/22/14 Pct Recovery = 59% Analysis Date = 08/22/14 Pct Recovery = 59% Analysis Date = 08/12/14 Pct Recovery = 59% Analysis Date = 08/12/14 Pct Recovery = 59% Analysis Date = 08/03/14 Pct Recovery = 59% Analysis Date = 08/03/14 Pct Recovery = 59% Analysis Date = 07/25/14 Pct Recovery = 59% Analysis Date = 07/25/14 Pct Recovery = 59% Analysis Date = 07/16/14 Pct Recovery = 60% Analysis Date = 07/16/14 Pct Recovery = 60% Analysis Date = 07/06/14 Pct Recovery = 60% Analysis Date = 07/06/14 Pct Recovery = 60% Analysis Date = 06/27/14 Pct Recovery = 60% Analysis Date = 06/27/14 Pct Recovery = 60% Analysis Date = 06/18/14 Pct Recovery = 60% Analysis Date = 06/18/14 Pct Recovery = 60% Analysis Date = 06/09/14 Pct Recovery = 60% Analysis Date = 06/09/14 Pct Recovery = 60% Analysis Date = 05/30/14 Pct Recovery = 61% Analysis Date = 05/30/14 Pct Recovery = 61% Analysis Date = 05/21/14 Pct Recovery = 61% Analysis Date = 05/21/14 Pct Recovery = 61% Analysis Date = 05/12/14 Pct Recovery = 61% Analysis Date = 05/12/14 Pct Recovery = 61% Analysis Date = 05/03/14 Pct Recovery = 62% Analysis Date = 05/03/14 Pct Recovery = 62% Analysis Date = 04/24/14 Pct Recovery = 62% Analysis Date = 04/24/14 Pct Recovery = 62% Analysis Date = 04/14/14 Pct Recovery = 62% Analysis Date = 04/14/14 Pct Recovery = 62% Analysis Date = 04/05/14 Pct Recovery = 62% Analysis Date = 04/05/14 Pct Recovery = 62% Analysis Date = 03/27/14 Pct Recovery = 62% Analysis Date = 03/27/14 Pct Recovery = 62% Analysis Date = 03/18/14 Pct Recovery = 62% Analysis Date = 03/18/14 Pct Recovery = 62% Analysis Date = 03/08/14 Pct Recovery = 61% Analysis Date = 03/08/14 Pct Recovery = 61% Analysis Date = 02/27/14 Pct Recovery = 60% Analysis Date = 02/27/14 Pct Recovery = 60% Analysis Date = 02/18/14 Pct Recovery = 60% Analysis Date = 02/18/14 Pct Recovery = 60% Analysis Date = 02/09/14 Pct Recovery = 59% Analysis Date = 02/09/14 Pct Recovery = 59% Analysis Date = 01/30/14 Pct Recovery = 59% Analysis Date = 01/30/14 Pct Recovery = 59% Analysis Date = 01/21/14 Pct Recovery = 58% Analysis Date = 01/21/14 Pct Recovery = 58% Analysis Date = 01/12/14 Pct Recovery = 58% Analysis Date = 01/12/14 Pct Recovery = 58% Analysis Date = 01/03/14 Pct Recovery = 57% Analysis Date = 01/03/14 Pct Recovery = 57% Analysis Date = 12/24/13 Pct Recovery = 57% Analysis Date = 12/24/13 Pct Recovery = 57% Analysis Date = 12/15/13 Pct Recovery = 57% Analysis Date = 12/15/13 Pct Recovery = 57% Analysis Date = 12/06/13 Pct Recovery = 56% Analysis Date = 12/06/13 Pct Recovery = 56% Analysis Date = 11/27/13 Pct Recovery = 56% Analysis Date = 11/27/13 Pct Recovery = 56% Analysis Date = 11/17/13 Pct Recovery = 55% Analysis Date = 11/17/13 Pct Recovery = 55% Analysis Date = 11/08/13 Pct Recovery = 55% Analysis Date = 11/08/13 Pct Recovery = 55% Analysis Date = 10/30/13 Pct Recovery = 55% Analysis Date = 10/30/13 Pct Recovery = 55% Analysis Date = 10/21/13 Pct Recovery = 54% Analysis Date = 10/21/13 Pct Recovery = 54% Analysis Date = 10/11/13 Pct Recovery = 54% Analysis Date = 10/11/13 Pct Recovery = 54% Analysis Date = 10/02/13 Pct Recovery = 54% Analysis Date = 10/02/13 Pct Recovery = 54% Analysis Date = 09/23/13 Pct Recovery = 53% Analysis Date = 09/23/13 Pct Recovery = 53% Analysis Date = 09/14/13 Pct Recovery = 53% Analysis Date = 09/14/13 Pct Recovery = 53% Analysis Date = 09/05/13 Pct Recovery = 53% Analysis Date = 09/05/13 Pct Recovery = 53% Analysis Date = 08/26/13 Pct Recovery = 52% Analysis Date = 08/26/13 Pct Recovery = 52% Analysis Date = 08/17/13 Pct Recovery = 52% Analysis Date = 08/17/13 Pct Recovery = 52% Analysis Date = 08/08/13 Pct Recovery = 52% Analysis Date = 08/08/13 Pct Recovery = 52% Analysis Date = 07/30/13 Pct Recovery = 51% Analysis Date = 07/30/13 Pct Recovery = 51% Analysis Date = 07/20/13 Pct Recovery = 51% Analysis Date = 07/20/13 Pct Recovery = 51% Analysis Date = 07/11/13 Pct Recovery = 51% Analysis Date = 07/11/13 Pct Recovery = 51% Analysis Date = 07/02/13 Pct Recovery = 50% Analysis Date = 07/02/13 Pct Recovery = 50% Analysis Date = 06/23/13 Pct Recovery = 50% Analysis Date = 06/23/13 Pct Recovery = 50% Analysis Date = 06/13/13 Pct Recovery = 50% Analysis Date = 06/13/13 Pct Recovery = 50% Analysis Date = 06/04/13 Pct Recovery = 49% Analysis Date = 06/04/13 Pct Recovery = 49% Analysis Date = 05/26/13 Pct Recovery = 49% Analysis Date = 05/26/13 Pct Recovery = 49% Analysis Date = 05/17/13 Pct Recovery = 49% Analysis Date = 05/17/13 Pct Recovery = 49% Analysis Date = 05/07/13 Pct Recovery = 48% Analysis Date = 05/07/13 Pct Recovery = 48% Analysis Date = 04/28/13 Pct Recovery = 48% Analysis Date = 04/28/13 Pct Recovery = 48% Analysis Date = 04/19/13 Pct Recovery = 48% Analysis Date = 04/19/13 Pct Recovery = 48% Analysis Date = 04/10/13 Pct Recovery = 47% Analysis Date = 04/10/13 Pct Recovery = 47% Analysis Date = 03/31/13 Pct Recovery = 47% Analysis Date = 03/31/13 Pct Recovery = 47% Analysis Date = 03/22/13 Pct Recovery = 47% Analysis Date = 03/22/13 Pct Recovery = 47% Analysis Date = 03/13/13 Pct Recovery = 46% Analysis Date = 03/13/13 Pct Recovery = 46% Analysis Date = 03/04/13 Pct Recovery = 46% Analysis Date = 03/04/13 Pct Recovery = 46% Analysis Date = 02/22/13 Pct Recovery = 46% Analysis Date = 02/22/13 Pct Recovery = 46% Analysis Date = 02/13/13 Pct Recovery = 45% Analysis Date = 02/13/13 Pct Recovery = 45% Analysis Date = 02/04/13 Pct Recovery = 45% Analysis Date = 02/04/13 Pct Recovery = 45% Analysis Date = 01/26/13 Pct Recovery = 45% Analysis Date = 01/26/13 Pct Recovery = 45% Analysis Date = 01/17/13 Pct Recovery = 44% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
PHORATE OXON

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 53 61% 19% 62% 15%
Total 53 61% 19% 62% 15%

Sample Statistics
PHORATE OXON

Characteristic N % % Basis
Plotted 53 95% Spiked
Estimated Values 53 95% Spiked
Deleted Values 7 6% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 61 .  
False Negatives 3 5% 3 out of 56
Not Spiked 57 .  
False Positives 0 0% 0 out of 55

OBSP Determination:
PHOSMET (IMIDAN)
METHOD: 2033 , TESTIDCODE: 61601GCM39

Laboratory ID = 20140100085 Lab Value = 1.190 Expected Conc. = 1.508 Report level label = 0.14 Pct Recovery = 79% Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl SpecificMix = 042413 Laboratory ID = 20172510330 Lab Value = 0.799 Expected Conc. = 0.936 Report level label = 0.14 Pct Recovery = 85% Analysis Date = 12/29/17 SpikeMix = ChemService 6537100: 100 µl & Abs 071817Pest: 100 µl SpecificMix = 6537100 Laboratory ID = 20162860079 Lab Value = 0.487 Expected Conc. = 0.872 Report level label = 0.14 Pct Recovery = 56% Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl SpecificMix = 060916 Laboratory ID = 20163150006 Lab Value = 0.498 Expected Conc. = 0.872 Report level label = 0.14 Pct Recovery = 57% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl SpecificMix = 060916 Laboratory ID = 20152750006 Lab Value = 0.389 Expected Conc. = 0.8408 Report level label = 0.14 Pct Recovery = 46% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl SpecificMix = 040615 Laboratory ID = 20152610011 Lab Value = 0.348 Expected Conc. = 0.8408 Report level label = 0.14 Pct Recovery = 41% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl SpecificMix = 040615 Laboratory ID = 20132690010 Lab Value = 0.601 Expected Conc. = 0.754 Report level label = 0.14 Pct Recovery = 80% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl SpecificMix = 042413 Laboratory ID = 20132560001 Lab Value = 0.435 Expected Conc. = 0.754 Report level label = 0.14 Pct Recovery = 58% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl SpecificMix = 042413 Laboratory ID = 20132140002 Lab Value = 0.448 Expected Conc. = 0.739 Report level label = 0.14 Pct Recovery = 61% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl SpecificMix = 04CC101 Laboratory ID = 20171380001 Lab Value = 0.294 Expected Conc. = 0.6984 Report level label = 0.14 Pct Recovery = 42% Analysis Date = 06/07/17 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 041816 Laboratory ID = 20170740063 Lab Value = 0.498 Expected Conc. = 0.6984 Report level label = 0.14 Pct Recovery = 71% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl SpecificMix = 041816 Laboratory ID = 20161740258 Lab Value = 0.406 Expected Conc. = 0.6984 Report level label = 0.14 Pct Recovery = 58% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 041816 Laboratory ID = 20171660002 Lab Value = 0.409 Expected Conc. = 0.6976 Report level label = 0.14 Pct Recovery = 59% Analysis Date = 08/23/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = 060916 Laboratory ID = 20170190026 Lab Value = 0.396 Expected Conc. = 0.6976 Report level label = 0.14 Pct Recovery = 57% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = 060916 Laboratory ID = 20150430092 Lab Value = 0.268 Expected Conc. = 0.5586 Report level label = 0.14 Pct Recovery = 48% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl SpecificMix = 042814 Laboratory ID = 20143240095 Lab Value = 0.391 Expected Conc. = 0.5586 Report level label = 0.14 Pct Recovery = 70% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl SpecificMix = 042814 Laboratory ID = 20142960086 Lab Value = 0.288 Expected Conc. = 0.5586 Report level label = 0.14 Pct Recovery = 52% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 042814 Laboratory ID = 20142530087 Lab Value = 0.205 Expected Conc. = 0.5586 Report level label = 0.14 Pct Recovery = 37% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl SpecificMix = 042814 Laboratory ID = 20150720069 Lab Value = 0.338 Expected Conc. = 0.552 Report level label = 0.14 Pct Recovery = 61% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 0227-14-08 Laboratory ID = 20141770149 Lab Value = 0.310 Expected Conc. = 0.552 Report level label = 0.14 Pct Recovery = 56% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl SpecificMix = 0227-14-08 Laboratory ID = 20141570088 Lab Value = 0.357 Expected Conc. = 0.552 Report level label = 0.14 Pct Recovery = 65% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl SpecificMix = 0227-14-08 Laboratory ID = 20130250061 Lab Value = 0.393 Expected Conc. = 0.49 Report level label = 0.14 Pct Recovery = 80% Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl SpecificMix = 05BB029 Laboratory ID = 20172230001 Lab Value = 0.368 Expected Conc. = 0.469 Report level label = 0.14 Pct Recovery = 78% Analysis Date = 10/19/17 SpikeMix = ChemService 6472100: 50 µl & Abs 071717Pest: 50 µl SpecificMix = 071717Pest Laboratory ID = 20172370001 Lab Value = 0.375 Expected Conc. = 0.468 Report level label = 0.14 Pct Recovery = 80% Analysis Date = 11/18/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6537100: 50 µl SpecificMix = 6537100 Laboratory ID = 20151900132 Lab Value = 0.212 Expected Conc. = 0.4204 Report level label = 0.14 Pct Recovery = 50% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl SpecificMix = 040615 Laboratory ID = 20151550293 Lab Value = 0.200 Expected Conc. = 0.4204 Report level label = 0.14 Pct Recovery = 48% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl SpecificMix = 040615 Laboratory ID = 20161260151 Lab Value = 0.205 Expected Conc. = 0.42 Report level label = 0.14 Pct Recovery = 49% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = EN150513008 Laboratory ID = 20160770090 Lab Value = 0.237 Expected Conc. = 0.42 Report level label = 0.14 Pct Recovery = 56% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = EN150513008 Laboratory ID = 20153510109 Lab Value = 0.223 Expected Conc. = 0.42 Report level label = 0.14 Pct Recovery = 53% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = EN150513008 Laboratory ID = 20152330039 Lab Value = 0.215 Expected Conc. = 0.42 Report level label = 0.14 Pct Recovery = 51% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl SpecificMix = EN150513008 Laboratory ID = 20172020035 Lab Value = 0.280 Expected Conc. = 0.3752 Report level label = 0.14 Pct Recovery = 75% Analysis Date = 11/07/17 SpikeMix = Abs 071717Pest: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 071717Pest Laboratory ID = 20171940002 Lab Value = 0.180 Expected Conc. = 0.3492 Report level label = 0.14 Pct Recovery = 52% Analysis Date = 11/10/17 SpikeMix = ChemService 5054800: 40 µl & NSI 041816: 40 µl SpecificMix = 041816 Laboratory ID = 20161600087 Lab Value = 0.207 Expected Conc. = 0.3492 Report level label = 0.14 Pct Recovery = 59% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 041816 Laboratory ID = 20161340228 Lab Value = 0.175 Expected Conc. = 0.3492 Report level label = 0.14 Pct Recovery = 50% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl SpecificMix = 041816 Laboratory ID = 20161190075 Lab Value = 0.164 Expected Conc. = 0.3492 Report level label = 0.14 Pct Recovery = 47% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 041816 Laboratory ID = 20171160110 Lab Value = 0.173 Expected Conc. = 0.3488 Report level label = 0.14 Pct Recovery = 50% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = 060916 Laboratory ID = 20162520001 Lab Value = 0.186 Expected Conc. = 0.3488 Report level label = 0.14 Pct Recovery = 53% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl SpecificMix = 060916 Laboratory ID = 20163560019 Lab Value = 0.176 Expected Conc. = 0.3488 Report level label = 0.14 Pct Recovery = 50% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl SpecificMix = 060916 Laboratory ID = 20162380004 Lab Value = 0.202 Expected Conc. = 0.3488 Report level label = 0.14 Pct Recovery = 58% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = 060916 Laboratory ID = 20133580036 Lab Value = 0.171 Expected Conc. = 0.3016 Report level label = 0.14 Pct Recovery = 57% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 042413 Laboratory ID = 20133190012 Lab Value = 0.222 Expected Conc. = 0.3016 Report level label = 0.14 Pct Recovery = 74% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 042413 Laboratory ID = 20131650073 Lab Value = 0.248 Expected Conc. = 0.3016 Report level label = 0.14 Pct Recovery = 82% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl SpecificMix = 042413 Laboratory ID = 20140730138 Lab Value = 0.163 Expected Conc. = 0.2956 Report level label = 0.14 Pct Recovery = 55% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 04CC101 Laboratory ID = 20140510043 Lab Value = 0.130 Expected Conc. = 0.2956 Report level label = 0.14 Pct Recovery = 44% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 04CC101 Laboratory ID = 20133310030 Lab Value = 0.235 Expected Conc. = 0.2956 Report level label = 0.14 Pct Recovery = 79% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl SpecificMix = 04CC101 Laboratory ID = 20132280016 Lab Value = 0.223 Expected Conc. = 0.2956 Report level label = 0.14 Pct Recovery = 75% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl SpecificMix = 04CC101 Laboratory ID = 20131510026 Lab Value = 0.156 Expected Conc. = 0.2956 Report level label = 0.14 Pct Recovery = 53% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl SpecificMix = 04CC101 Laboratory ID = 20173120093 Lab Value = 0.199 Expected Conc. = 0.2808 Report level label = 0.14 Pct Recovery = 71% Analysis Date = 03/10/18 SpikeMix = ChemService 6472100: 30 µl & ChemService 6537100: 30 µl SpecificMix = 6537100 Laboratory ID = 20172780018 Lab Value = 0.167 Expected Conc. = 0.2808 Report level label = 0.14 Pct Recovery = 59% Analysis Date = 02/08/18 SpikeMix = ChemService 6537100: 30 µl & Abs 071817Pest: 30 µl SpecificMix = 6537100 Laboratory ID = 20143370094 Lab Value = 0.128 Expected Conc. = 0.2793 Report level label = 0.14 Pct Recovery = 46% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl SpecificMix = 042814 Laboratory ID = 20142820151 Lab Value = 0.166 Expected Conc. = 0.2793 Report level label = 0.14 Pct Recovery = 59% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl SpecificMix = 042814 Laboratory ID = 20142470041 Lab Value = 0.147 Expected Conc. = 0.2793 Report level label = 0.14 Pct Recovery = 53% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl SpecificMix = 042814 Laboratory ID = 20142200164 Lab Value = 0.129 Expected Conc. = 0.2793 Report level label = 0.14 Pct Recovery = 46% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 042814 Laboratory ID = 20141840097 Lab Value = 0.109 Expected Conc. = 0.276 Report level label = 0.14 Pct Recovery = 39% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20141490205 Lab Value = 0.168 Expected Conc. = 0.276 Report level label = 0.14 Pct Recovery = 61% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20141420140 Lab Value = 0.203 Expected Conc. = 0.276 Report level label = 0.14 Pct Recovery = 74% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20141360094 Lab Value = 0.133 Expected Conc. = 0.276 Report level label = 0.14 Pct Recovery = 48% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20130940097 Lab Value = 0.133 Expected Conc. = 0.251 Report level label = 0.14 Pct Recovery = 53% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = 052412 Laboratory ID = 20130100066 Lab Value = 0.222 Expected Conc. = 0.251 Report level label = 0.14 Pct Recovery = 88% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl SpecificMix = 052412 Laboratory ID = 20140230082 Lab Value = 0.138 Expected Conc. = 0.2505 Report level label = 0.14 Pct Recovery = 55% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl SpecificMix = 012513 Laboratory ID = 20132420001 Lab Value = 0.170 Expected Conc. = 0.2505 Report level label = 0.14 Pct Recovery = 68% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl SpecificMix = 012513 Laboratory ID = 20161050143 Lab Value = 0.119 Expected Conc. = 0.2102 Report level label = 0.14 Pct Recovery = 57% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Laboratory ID = 20160430111 Lab Value = 0.115 Expected Conc. = 0.2102 Report level label = 0.14 Pct Recovery = 55% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Laboratory ID = 20160070059 Lab Value = 0.103 Expected Conc. = 0.2102 Report level label = 0.14 Pct Recovery = 49% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = 040615 Laboratory ID = 20151380009 Lab Value = 0.101 Expected Conc. = 0.2102 Report level label = 0.14 Pct Recovery = 48% Analysis Date = 05/30/15 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Laboratory ID = 20151210037 Lab Value = 0.108 Expected Conc. = 0.2102 Report level label = 0.14 Pct Recovery = 51% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Laboratory ID = 20160560044 Lab Value = 0.105 Expected Conc. = 0.21 Report level label = 0.14 Pct Recovery = 50% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl SpecificMix = EN150513008 Laboratory ID = 20153160001 Lab Value = 0.102 Expected Conc. = 0.21 Report level label = 0.14 Pct Recovery = 49% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = EN150513008 Laboratory ID = 20153030068 Lab Value = 0.115 Expected Conc. = 0.21 Report level label = 0.14 Pct Recovery = 55% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150513008 Laboratory ID = 20152190003 Lab Value = 0.098 Expected Conc. = 0.21 Report level label = 0.14 Pct Recovery = 47% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150513008 Laboratory ID = 20151480170 Lab Value = 0.129 Expected Conc. = 0.21 Report level label = 0.14 Pct Recovery = 61% Analysis Date = 06/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150513008 Laboratory ID = 20133400002 Lab Value = 0.074 Expected Conc. = 0.1004 Report level label = 0.14 Pct Recovery = 74% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = 052412 Laboratory ID = 20132910008 Lab Value = 0.057 Expected Conc. = 0.1004 Report level label = 0.14 Pct Recovery = 57% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = 052412 Laboratory ID = 20130650005 Lab Value = 0.057 Expected Conc. = 0.1004 Report level label = 0.14 Pct Recovery = 57% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl SpecificMix = 052412 Laboratory ID = 20140860102 Lab Value = 0.044 Expected Conc. = 0.1002 Report level label = 0.14 Pct Recovery = 44% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 012513 Laboratory ID = 20131920149 Lab Value = 0.068 Expected Conc. = 0.1002 Report level label = 0.14 Pct Recovery = 68% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl SpecificMix = 012513 Laboratory ID = 20131230084 Lab Value = 0.088 Expected Conc. = 0.098 Report level label = 0.14 Pct Recovery = 90% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl SpecificMix = 05BB029 Laboratory ID = 20130510051 Lab Value = 0.088 Expected Conc. = 0.098 Report level label = 0.14 Pct Recovery = 90% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl SpecificMix = 05BB029 Analysis Date = 03/09/18 Pct Recovery = 69% Analysis Date = 02/28/18 Pct Recovery = 68% Analysis Date = 02/28/18 Pct Recovery = 68% Analysis Date = 02/19/18 Pct Recovery = 68% Analysis Date = 02/19/18 Pct Recovery = 68% Analysis Date = 02/09/18 Pct Recovery = 68% Analysis Date = 02/09/18 Pct Recovery = 68% Analysis Date = 01/31/18 Pct Recovery = 68% Analysis Date = 01/31/18 Pct Recovery = 68% Analysis Date = 01/22/18 Pct Recovery = 68% Analysis Date = 01/22/18 Pct Recovery = 68% Analysis Date = 01/12/18 Pct Recovery = 67% Analysis Date = 01/12/18 Pct Recovery = 67% Analysis Date = 01/03/18 Pct Recovery = 67% Analysis Date = 01/03/18 Pct Recovery = 67% Analysis Date = 12/24/17 Pct Recovery = 67% Analysis Date = 12/24/17 Pct Recovery = 67% Analysis Date = 12/15/17 Pct Recovery = 67% Analysis Date = 12/15/17 Pct Recovery = 67% Analysis Date = 12/06/17 Pct Recovery = 66% Analysis Date = 12/06/17 Pct Recovery = 66% Analysis Date = 11/26/17 Pct Recovery = 66% Analysis Date = 11/26/17 Pct Recovery = 66% Analysis Date = 11/17/17 Pct Recovery = 66% Analysis Date = 11/17/17 Pct Recovery = 66% Analysis Date = 11/07/17 Pct Recovery = 66% Analysis Date = 11/07/17 Pct Recovery = 66% Analysis Date = 10/29/17 Pct Recovery = 65% Analysis Date = 10/29/17 Pct Recovery = 65% Analysis Date = 10/20/17 Pct Recovery = 65% Analysis Date = 10/20/17 Pct Recovery = 65% Analysis Date = 10/10/17 Pct Recovery = 65% Analysis Date = 10/10/17 Pct Recovery = 65% Analysis Date = 10/01/17 Pct Recovery = 65% Analysis Date = 10/01/17 Pct Recovery = 65% Analysis Date = 09/21/17 Pct Recovery = 64% Analysis Date = 09/21/17 Pct Recovery = 64% Analysis Date = 09/12/17 Pct Recovery = 64% Analysis Date = 09/12/17 Pct Recovery = 64% Analysis Date = 09/03/17 Pct Recovery = 64% Analysis Date = 09/03/17 Pct Recovery = 64% Analysis Date = 08/24/17 Pct Recovery = 64% Analysis Date = 08/24/17 Pct Recovery = 64% Analysis Date = 08/15/17 Pct Recovery = 64% Analysis Date = 08/15/17 Pct Recovery = 64% Analysis Date = 08/06/17 Pct Recovery = 63% Analysis Date = 08/06/17 Pct Recovery = 63% Analysis Date = 07/27/17 Pct Recovery = 63% Analysis Date = 07/27/17 Pct Recovery = 63% Analysis Date = 07/18/17 Pct Recovery = 63% Analysis Date = 07/18/17 Pct Recovery = 63% Analysis Date = 07/08/17 Pct Recovery = 63% Analysis Date = 07/08/17 Pct Recovery = 63% Analysis Date = 06/29/17 Pct Recovery = 62% Analysis Date = 06/29/17 Pct Recovery = 62% Analysis Date = 06/20/17 Pct Recovery = 62% Analysis Date = 06/20/17 Pct Recovery = 62% Analysis Date = 06/10/17 Pct Recovery = 62% Analysis Date = 06/10/17 Pct Recovery = 62% Analysis Date = 06/01/17 Pct Recovery = 62% Analysis Date = 06/01/17 Pct Recovery = 62% Analysis Date = 05/22/17 Pct Recovery = 61% Analysis Date = 05/22/17 Pct Recovery = 61% Analysis Date = 05/13/17 Pct Recovery = 61% Analysis Date = 05/13/17 Pct Recovery = 61% Analysis Date = 05/04/17 Pct Recovery = 61% Analysis Date = 05/04/17 Pct Recovery = 61% Analysis Date = 04/24/17 Pct Recovery = 61% Analysis Date = 04/24/17 Pct Recovery = 61% Analysis Date = 04/15/17 Pct Recovery = 61% Analysis Date = 04/15/17 Pct Recovery = 61% Analysis Date = 04/05/17 Pct Recovery = 60% Analysis Date = 04/05/17 Pct Recovery = 60% Analysis Date = 03/27/17 Pct Recovery = 60% Analysis Date = 03/27/17 Pct Recovery = 60% Analysis Date = 03/18/17 Pct Recovery = 60% Analysis Date = 03/18/17 Pct Recovery = 60% Analysis Date = 03/08/17 Pct Recovery = 60% Analysis Date = 03/08/17 Pct Recovery = 60% Analysis Date = 02/27/17 Pct Recovery = 59% Analysis Date = 02/27/17 Pct Recovery = 59% Analysis Date = 02/18/17 Pct Recovery = 59% Analysis Date = 02/18/17 Pct Recovery = 59% Analysis Date = 02/08/17 Pct Recovery = 59% Analysis Date = 02/08/17 Pct Recovery = 59% Analysis Date = 01/30/17 Pct Recovery = 59% Analysis Date = 01/30/17 Pct Recovery = 59% Analysis Date = 01/20/17 Pct Recovery = 59% Analysis Date = 01/20/17 Pct Recovery = 59% Analysis Date = 01/11/17 Pct Recovery = 58% Analysis Date = 01/11/17 Pct Recovery = 58% Analysis Date = 01/02/17 Pct Recovery = 58% Analysis Date = 01/02/17 Pct Recovery = 58% Analysis Date = 12/23/16 Pct Recovery = 58% Analysis Date = 12/23/16 Pct Recovery = 58% Analysis Date = 12/14/16 Pct Recovery = 58% Analysis Date = 12/14/16 Pct Recovery = 58% Analysis Date = 12/04/16 Pct Recovery = 57% Analysis Date = 12/04/16 Pct Recovery = 57% Analysis Date = 11/25/16 Pct Recovery = 57% Analysis Date = 11/25/16 Pct Recovery = 57% Analysis Date = 11/16/16 Pct Recovery = 57% Analysis Date = 11/16/16 Pct Recovery = 57% Analysis Date = 11/06/16 Pct Recovery = 57% Analysis Date = 11/06/16 Pct Recovery = 57% Analysis Date = 10/28/16 Pct Recovery = 57% Analysis Date = 10/28/16 Pct Recovery = 57% Analysis Date = 10/18/16 Pct Recovery = 56% Analysis Date = 10/18/16 Pct Recovery = 56% Analysis Date = 10/09/16 Pct Recovery = 56% Analysis Date = 10/09/16 Pct Recovery = 56% Analysis Date = 09/30/16 Pct Recovery = 56% Analysis Date = 09/30/16 Pct Recovery = 56% Analysis Date = 09/20/16 Pct Recovery = 56% Analysis Date = 09/20/16 Pct Recovery = 56% Analysis Date = 09/11/16 Pct Recovery = 55% Analysis Date = 09/11/16 Pct Recovery = 55% Analysis Date = 09/01/16 Pct Recovery = 55% Analysis Date = 09/01/16 Pct Recovery = 55% Analysis Date = 08/23/16 Pct Recovery = 55% Analysis Date = 08/23/16 Pct Recovery = 55% Analysis Date = 08/14/16 Pct Recovery = 55% Analysis Date = 08/14/16 Pct Recovery = 55% Analysis Date = 08/04/16 Pct Recovery = 55% Analysis Date = 08/04/16 Pct Recovery = 55% Analysis Date = 07/26/16 Pct Recovery = 54% Analysis Date = 07/26/16 Pct Recovery = 54% Analysis Date = 07/17/16 Pct Recovery = 54% Analysis Date = 07/17/16 Pct Recovery = 54% Analysis Date = 07/07/16 Pct Recovery = 54% Analysis Date = 07/07/16 Pct Recovery = 54% Analysis Date = 06/28/16 Pct Recovery = 54% Analysis Date = 06/28/16 Pct Recovery = 54% Analysis Date = 06/18/16 Pct Recovery = 54% Analysis Date = 06/18/16 Pct Recovery = 54% Analysis Date = 06/09/16 Pct Recovery = 53% Analysis Date = 06/09/16 Pct Recovery = 53% Analysis Date = 05/31/16 Pct Recovery = 53% Analysis Date = 05/31/16 Pct Recovery = 53% Analysis Date = 05/21/16 Pct Recovery = 53% Analysis Date = 05/21/16 Pct Recovery = 53% Analysis Date = 05/12/16 Pct Recovery = 53% Analysis Date = 05/12/16 Pct Recovery = 53% Analysis Date = 05/02/16 Pct Recovery = 53% Analysis Date = 05/02/16 Pct Recovery = 53% Analysis Date = 04/23/16 Pct Recovery = 53% Analysis Date = 04/23/16 Pct Recovery = 53% Analysis Date = 04/14/16 Pct Recovery = 53% Analysis Date = 04/14/16 Pct Recovery = 53% Analysis Date = 04/04/16 Pct Recovery = 53% Analysis Date = 04/04/16 Pct Recovery = 53% Analysis Date = 03/26/16 Pct Recovery = 53% Analysis Date = 03/26/16 Pct Recovery = 53% Analysis Date = 03/16/16 Pct Recovery = 52% Analysis Date = 03/16/16 Pct Recovery = 52% Analysis Date = 03/07/16 Pct Recovery = 52% Analysis Date = 03/07/16 Pct Recovery = 52% Analysis Date = 02/27/16 Pct Recovery = 52% Analysis Date = 02/27/16 Pct Recovery = 52% Analysis Date = 02/17/16 Pct Recovery = 52% Analysis Date = 02/17/16 Pct Recovery = 52% Analysis Date = 02/08/16 Pct Recovery = 52% Analysis Date = 02/08/16 Pct Recovery = 52% Analysis Date = 01/30/16 Pct Recovery = 52% Analysis Date = 01/30/16 Pct Recovery = 52% Analysis Date = 01/20/16 Pct Recovery = 52% Analysis Date = 01/20/16 Pct Recovery = 52% Analysis Date = 01/11/16 Pct Recovery = 52% Analysis Date = 01/11/16 Pct Recovery = 52% Analysis Date = 01/01/16 Pct Recovery = 52% Analysis Date = 01/01/16 Pct Recovery = 52% Analysis Date = 12/23/15 Pct Recovery = 52% Analysis Date = 12/23/15 Pct Recovery = 52% Analysis Date = 12/14/15 Pct Recovery = 52% Analysis Date = 12/14/15 Pct Recovery = 52% Analysis Date = 12/04/15 Pct Recovery = 52% Analysis Date = 12/04/15 Pct Recovery = 52% Analysis Date = 11/25/15 Pct Recovery = 52% Analysis Date = 11/25/15 Pct Recovery = 52% Analysis Date = 11/15/15 Pct Recovery = 52% Analysis Date = 11/15/15 Pct Recovery = 52% Analysis Date = 11/06/15 Pct Recovery = 52% Analysis Date = 11/06/15 Pct Recovery = 52% Analysis Date = 10/28/15 Pct Recovery = 52% Analysis Date = 10/28/15 Pct Recovery = 52% Analysis Date = 10/18/15 Pct Recovery = 52% Analysis Date = 10/18/15 Pct Recovery = 52% Analysis Date = 10/09/15 Pct Recovery = 52% Analysis Date = 10/09/15 Pct Recovery = 52% Analysis Date = 09/29/15 Pct Recovery = 52% Analysis Date = 09/29/15 Pct Recovery = 52% Analysis Date = 09/20/15 Pct Recovery = 52% Analysis Date = 09/20/15 Pct Recovery = 52% Analysis Date = 09/11/15 Pct Recovery = 52% Analysis Date = 09/11/15 Pct Recovery = 52% Analysis Date = 09/01/15 Pct Recovery = 52% Analysis Date = 09/01/15 Pct Recovery = 52% Analysis Date = 08/23/15 Pct Recovery = 52% Analysis Date = 08/23/15 Pct Recovery = 52% Analysis Date = 08/13/15 Pct Recovery = 52% Analysis Date = 08/13/15 Pct Recovery = 52% Analysis Date = 08/04/15 Pct Recovery = 52% Analysis Date = 08/04/15 Pct Recovery = 52% Analysis Date = 07/26/15 Pct Recovery = 52% Analysis Date = 07/26/15 Pct Recovery = 52% Analysis Date = 07/16/15 Pct Recovery = 52% Analysis Date = 07/16/15 Pct Recovery = 52% Analysis Date = 07/07/15 Pct Recovery = 52% Analysis Date = 07/07/15 Pct Recovery = 52% Analysis Date = 06/28/15 Pct Recovery = 52% Analysis Date = 06/28/15 Pct Recovery = 52% Analysis Date = 06/18/15 Pct Recovery = 52% Analysis Date = 06/18/15 Pct Recovery = 52% Analysis Date = 06/09/15 Pct Recovery = 52% Analysis Date = 06/09/15 Pct Recovery = 52% Analysis Date = 05/30/15 Pct Recovery = 52% Analysis Date = 05/30/15 Pct Recovery = 52% Analysis Date = 05/21/15 Pct Recovery = 52% Analysis Date = 05/21/15 Pct Recovery = 52% Analysis Date = 05/12/15 Pct Recovery = 52% Analysis Date = 05/12/15 Pct Recovery = 52% Analysis Date = 05/02/15 Pct Recovery = 52% Analysis Date = 05/02/15 Pct Recovery = 52% Analysis Date = 04/23/15 Pct Recovery = 52% Analysis Date = 04/23/15 Pct Recovery = 52% Analysis Date = 04/13/15 Pct Recovery = 52% Analysis Date = 04/13/15 Pct Recovery = 52% Analysis Date = 04/04/15 Pct Recovery = 52% Analysis Date = 04/04/15 Pct Recovery = 52% Analysis Date = 03/26/15 Pct Recovery = 52% Analysis Date = 03/26/15 Pct Recovery = 52% Analysis Date = 03/16/15 Pct Recovery = 52% Analysis Date = 03/16/15 Pct Recovery = 52% Analysis Date = 03/07/15 Pct Recovery = 52% Analysis Date = 03/07/15 Pct Recovery = 52% Analysis Date = 02/25/15 Pct Recovery = 53% Analysis Date = 02/25/15 Pct Recovery = 53% Analysis Date = 02/16/15 Pct Recovery = 53% Analysis Date = 02/16/15 Pct Recovery = 53% Analysis Date = 02/07/15 Pct Recovery = 53% Analysis Date = 02/07/15 Pct Recovery = 53% Analysis Date = 01/28/15 Pct Recovery = 53% Analysis Date = 01/28/15 Pct Recovery = 53% Analysis Date = 01/19/15 Pct Recovery = 53% Analysis Date = 01/19/15 Pct Recovery = 53% Analysis Date = 01/10/15 Pct Recovery = 54% Analysis Date = 01/10/15 Pct Recovery = 54% Analysis Date = 12/31/14 Pct Recovery = 54% Analysis Date = 12/31/14 Pct Recovery = 54% Analysis Date = 12/22/14 Pct Recovery = 54% Analysis Date = 12/22/14 Pct Recovery = 54% Analysis Date = 12/12/14 Pct Recovery = 54% Analysis Date = 12/12/14 Pct Recovery = 54% Analysis Date = 12/03/14 Pct Recovery = 54% Analysis Date = 12/03/14 Pct Recovery = 54% Analysis Date = 11/24/14 Pct Recovery = 54% Analysis Date = 11/24/14 Pct Recovery = 54% Analysis Date = 11/14/14 Pct Recovery = 55% Analysis Date = 11/14/14 Pct Recovery = 55% Analysis Date = 11/05/14 Pct Recovery = 55% Analysis Date = 11/05/14 Pct Recovery = 55% Analysis Date = 10/26/14 Pct Recovery = 55% Analysis Date = 10/26/14 Pct Recovery = 55% Analysis Date = 10/17/14 Pct Recovery = 55% Analysis Date = 10/17/14 Pct Recovery = 55% Analysis Date = 10/08/14 Pct Recovery = 55% Analysis Date = 10/08/14 Pct Recovery = 55% Analysis Date = 09/28/14 Pct Recovery = 56% Analysis Date = 09/28/14 Pct Recovery = 56% Analysis Date = 09/19/14 Pct Recovery = 56% Analysis Date = 09/19/14 Pct Recovery = 56% Analysis Date = 09/09/14 Pct Recovery = 56% Analysis Date = 09/09/14 Pct Recovery = 56% Analysis Date = 08/31/14 Pct Recovery = 56% Analysis Date = 08/31/14 Pct Recovery = 56% Analysis Date = 08/22/14 Pct Recovery = 56% Analysis Date = 08/22/14 Pct Recovery = 56% Analysis Date = 08/12/14 Pct Recovery = 56% Analysis Date = 08/12/14 Pct Recovery = 56% Analysis Date = 08/03/14 Pct Recovery = 57% Analysis Date = 08/03/14 Pct Recovery = 57% Analysis Date = 07/25/14 Pct Recovery = 57% Analysis Date = 07/25/14 Pct Recovery = 57% Analysis Date = 07/15/14 Pct Recovery = 57% Analysis Date = 07/15/14 Pct Recovery = 57% Analysis Date = 07/06/14 Pct Recovery = 57% Analysis Date = 07/06/14 Pct Recovery = 57% Analysis Date = 06/26/14 Pct Recovery = 57% Analysis Date = 06/26/14 Pct Recovery = 57% Analysis Date = 06/17/14 Pct Recovery = 58% Analysis Date = 06/17/14 Pct Recovery = 58% Analysis Date = 06/08/14 Pct Recovery = 58% Analysis Date = 06/08/14 Pct Recovery = 58% Analysis Date = 05/29/14 Pct Recovery = 58% Analysis Date = 05/29/14 Pct Recovery = 58% Analysis Date = 05/20/14 Pct Recovery = 58% Analysis Date = 05/20/14 Pct Recovery = 58% Analysis Date = 05/10/14 Pct Recovery = 59% Analysis Date = 05/10/14 Pct Recovery = 59% Analysis Date = 05/01/14 Pct Recovery = 59% Analysis Date = 05/01/14 Pct Recovery = 59% Analysis Date = 04/22/14 Pct Recovery = 59% Analysis Date = 04/22/14 Pct Recovery = 59% Analysis Date = 04/12/14 Pct Recovery = 60% Analysis Date = 04/12/14 Pct Recovery = 60% Analysis Date = 04/03/14 Pct Recovery = 60% Analysis Date = 04/03/14 Pct Recovery = 60% Analysis Date = 03/24/14 Pct Recovery = 60% Analysis Date = 03/24/14 Pct Recovery = 60% Analysis Date = 03/15/14 Pct Recovery = 61% Analysis Date = 03/15/14 Pct Recovery = 61% Analysis Date = 03/06/14 Pct Recovery = 61% Analysis Date = 03/06/14 Pct Recovery = 61% Analysis Date = 02/24/14 Pct Recovery = 61% Analysis Date = 02/24/14 Pct Recovery = 61% Analysis Date = 02/15/14 Pct Recovery = 62% Analysis Date = 02/15/14 Pct Recovery = 62% Analysis Date = 02/05/14 Pct Recovery = 62% Analysis Date = 02/05/14 Pct Recovery = 62% Analysis Date = 01/27/14 Pct Recovery = 62% Analysis Date = 01/27/14 Pct Recovery = 62% Analysis Date = 01/18/14 Pct Recovery = 63% Analysis Date = 01/18/14 Pct Recovery = 63% Analysis Date = 01/08/14 Pct Recovery = 63% Analysis Date = 01/08/14 Pct Recovery = 63% Analysis Date = 12/30/13 Pct Recovery = 63% Analysis Date = 12/30/13 Pct Recovery = 63% Analysis Date = 12/21/13 Pct Recovery = 64% Analysis Date = 12/21/13 Pct Recovery = 64% Analysis Date = 12/11/13 Pct Recovery = 64% Analysis Date = 12/11/13 Pct Recovery = 64% Analysis Date = 12/02/13 Pct Recovery = 64% Analysis Date = 12/02/13 Pct Recovery = 64% Analysis Date = 11/22/13 Pct Recovery = 65% Analysis Date = 11/22/13 Pct Recovery = 65% Analysis Date = 11/13/13 Pct Recovery = 65% Analysis Date = 11/13/13 Pct Recovery = 65% Analysis Date = 11/04/13 Pct Recovery = 66% Analysis Date = 11/04/13 Pct Recovery = 66% Analysis Date = 10/25/13 Pct Recovery = 66% Analysis Date = 10/25/13 Pct Recovery = 66% Analysis Date = 10/16/13 Pct Recovery = 66% Analysis Date = 10/16/13 Pct Recovery = 66% Analysis Date = 10/06/13 Pct Recovery = 67% Analysis Date = 10/06/13 Pct Recovery = 67% Analysis Date = 09/27/13 Pct Recovery = 67% Analysis Date = 09/27/13 Pct Recovery = 67% Analysis Date = 09/18/13 Pct Recovery = 68% Analysis Date = 09/18/13 Pct Recovery = 68% Analysis Date = 09/08/13 Pct Recovery = 68% Analysis Date = 09/08/13 Pct Recovery = 68% Analysis Date = 08/30/13 Pct Recovery = 68% Analysis Date = 08/30/13 Pct Recovery = 68% Analysis Date = 08/20/13 Pct Recovery = 69% Analysis Date = 08/20/13 Pct Recovery = 69% Analysis Date = 08/11/13 Pct Recovery = 69% Analysis Date = 08/11/13 Pct Recovery = 69% Analysis Date = 08/02/13 Pct Recovery = 70% Analysis Date = 08/02/13 Pct Recovery = 70% Analysis Date = 07/23/13 Pct Recovery = 70% Analysis Date = 07/23/13 Pct Recovery = 70% Analysis Date = 07/14/13 Pct Recovery = 70% Analysis Date = 07/14/13 Pct Recovery = 70% Analysis Date = 07/05/13 Pct Recovery = 71% Analysis Date = 07/05/13 Pct Recovery = 71% Analysis Date = 06/25/13 Pct Recovery = 71% Analysis Date = 06/25/13 Pct Recovery = 71% Analysis Date = 06/16/13 Pct Recovery = 72% Analysis Date = 06/16/13 Pct Recovery = 72% Analysis Date = 06/06/13 Pct Recovery = 72% Analysis Date = 06/06/13 Pct Recovery = 72% Analysis Date = 05/28/13 Pct Recovery = 72% Analysis Date = 05/28/13 Pct Recovery = 72% Analysis Date = 05/19/13 Pct Recovery = 73% Analysis Date = 05/19/13 Pct Recovery = 73% Analysis Date = 05/09/13 Pct Recovery = 73% Analysis Date = 05/09/13 Pct Recovery = 73% Analysis Date = 04/30/13 Pct Recovery = 74% Analysis Date = 04/30/13 Pct Recovery = 74% Analysis Date = 04/20/13 Pct Recovery = 74% Analysis Date = 04/20/13 Pct Recovery = 74% Analysis Date = 04/11/13 Pct Recovery = 74% Analysis Date = 04/11/13 Pct Recovery = 74% Analysis Date = 04/02/13 Pct Recovery = 75% Analysis Date = 04/02/13 Pct Recovery = 75% Analysis Date = 03/23/13 Pct Recovery = 75% Analysis Date = 03/23/13 Pct Recovery = 75% Analysis Date = 03/14/13 Pct Recovery = 76% Analysis Date = 03/14/13 Pct Recovery = 76% Analysis Date = 03/04/13 Pct Recovery = 76% Analysis Date = 03/04/13 Pct Recovery = 76% Analysis Date = 02/23/13 Pct Recovery = 76% Analysis Date = 02/23/13 Pct Recovery = 76% Analysis Date = 02/14/13 Pct Recovery = 77% Analysis Date = 02/14/13 Pct Recovery = 77% Analysis Date = 02/04/13 Pct Recovery = 77% Analysis Date = 02/04/13 Pct Recovery = 77% Analysis Date = 01/26/13 Pct Recovery = 78% Analysis Date = 01/26/13 Pct Recovery = 78% Analysis Date = 01/17/13 Pct Recovery = 78% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
PHOSMET (IMIDAN)

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 7 68% 17% 68% 24%
>= Reporting Level 71 58% 12% 56% 11%
Total 78 59% 13% 57% 13%

Sample Statistics
PHOSMET (IMIDAN)

Characteristic N % % Basis
Plotted 78 100% Spiked
Estimated Values 78 100% Spiked
Deleted Values 2 2% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 79 .  
False Negatives 0 0% 0 out of 78
Not Spiked 39 .  
False Positives 0 0% 0 out of 38

OBSP Determination:
PHOSMET OXON
METHOD: 2033 , TESTIDCODE: 61668GCM39

Laboratory ID = 20140100085 Lab Value = 0.309 Expected Conc. = 0.5 Report level label = 0.0511 Pct Recovery = 62% Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl SpecificMix = 042413 Laboratory ID = 20130250061 Lab Value = 0.273 Expected Conc. = 0.371 Report level label = 0.0511 Pct Recovery = 74% Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl SpecificMix = 05BB029 Laboratory ID = 20172510330 Lab Value = 0.205 Expected Conc. = 0.341 Report level label = 0.0511 Pct Recovery = 60% Analysis Date = 12/29/17 SpikeMix = ChemService 6537100: 100 µl & Abs 071817Pest: 100 µl SpecificMix = 6537100 Laboratory ID = 20152610011 Lab Value = 0.107 Expected Conc. = 0.3064 Report level label = 0.0511 Pct Recovery = 35% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl SpecificMix = 0406-15-01 Laboratory ID = 20152460215 Lab Value = 0.200 Expected Conc. = 0.3064 Report level label = 0.0511 Pct Recovery = 65% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl SpecificMix = 0406-15-01 Laboratory ID = 20172020035 Lab Value = 0.208 Expected Conc. = 0.2624 Report level label = 0.0511 Pct Recovery = 79% Analysis Date = 11/07/17 SpikeMix = Abs 071717Pest: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20170960001 Lab Value = 0.154 Expected Conc. = 0.2528 Report level label = 0.0511 Pct Recovery = 61% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl SpecificMix = 03FF076 Laboratory ID = 20132690010 Lab Value = 0.173 Expected Conc. = 0.25 Report level label = 0.0511 Pct Recovery = 69% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl SpecificMix = 042413 Laboratory ID = 20132560001 Lab Value = 0.077 Expected Conc. = 0.25 Report level label = 0.0511 Pct Recovery = 31% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl SpecificMix = 042413 Laboratory ID = 20132140002 Lab Value = 0.076 Expected Conc. = 0.2485 Report level label = 0.0511 Pct Recovery = 31% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl SpecificMix = 04CC101 Laboratory ID = 20150720069 Lab Value = 0.059 Expected Conc. = 0.2028 Report level label = 0.0511 Pct Recovery = 29% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 0227-14-08 Laboratory ID = 20141770149 Lab Value = 0.114 Expected Conc. = 0.2028 Report level label = 0.0511 Pct Recovery = 56% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl SpecificMix = 0227-14-08 Laboratory ID = 20141570088 Lab Value = 0.113 Expected Conc. = 0.2028 Report level label = 0.0511 Pct Recovery = 56% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl SpecificMix = 0227-14-08 Laboratory ID = 20140230082 Lab Value = 0.132 Expected Conc. = 0.188 Report level label = 0.0511 Pct Recovery = 70% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl SpecificMix = 012513 Laboratory ID = 20132420001 Lab Value = 0.127 Expected Conc. = 0.188 Report level label = 0.0511 Pct Recovery = 68% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl SpecificMix = 012513 Laboratory ID = 20130940097 Lab Value = 0.098 Expected Conc. = 0.188 Report level label = 0.0511 Pct Recovery = 52% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = 052412 Laboratory ID = 20130100066 Lab Value = 0.190 Expected Conc. = 0.188 Report level label = 0.0511 Pct Recovery = 101% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl SpecificMix = 052412 Laboratory ID = 20172370001 Lab Value = 0.186 Expected Conc. = 0.1705 Report level label = 0.0511 Pct Recovery = 109% Analysis Date = 11/18/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6537100: 50 µl SpecificMix = 6537100 Laboratory ID = 20172230001 Lab Value = 0.128 Expected Conc. = 0.17 Report level label = 0.0511 Pct Recovery = 75% Analysis Date = 10/19/17 SpikeMix = ChemService 6472100: 50 µl & Abs 071717Pest: 50 µl SpecificMix = 071717Pest Laboratory ID = 20160770090 Lab Value = 0.125 Expected Conc. = 0.1532 Report level label = 0.0511 Pct Recovery = 82% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20160630046 Lab Value = 0.124 Expected Conc. = 0.1532 Report level label = 0.0511 Pct Recovery = 81% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20153510109 Lab Value = 0.093 Expected Conc. = 0.1532 Report level label = 0.0511 Pct Recovery = 61% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20153440001 Lab Value = 0.097 Expected Conc. = 0.1532 Report level label = 0.0511 Pct Recovery = 63% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20161260151 Lab Value = 0.096 Expected Conc. = 0.152 Report level label = 0.0511 Pct Recovery = 63% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = 3851600 Laboratory ID = 20151550293 Lab Value = 0.097 Expected Conc. = 0.152 Report level label = 0.0511 Pct Recovery = 63% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl SpecificMix = 3851600 Laboratory ID = 20151270112 Lab Value = 0.085 Expected Conc. = 0.152 Report level label = 0.0511 Pct Recovery = 56% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl SpecificMix = 3851600 Laboratory ID = 20171510080 Lab Value = 0.102 Expected Conc. = 0.1264 Report level label = 0.0511 Pct Recovery = 81% Analysis Date = 06/09/17 SpikeMix = Supelco LC20138V: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20170460061 Lab Value = 0.092 Expected Conc. = 0.1264 Report level label = 0.0511 Pct Recovery = 73% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl SpecificMix = 03FF076 Laboratory ID = 20162660005 Lab Value = 0.097 Expected Conc. = 0.1264 Report level label = 0.0511 Pct Recovery = 76% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl SpecificMix = 03FF076 Laboratory ID = 20161340228 Lab Value = 0.085 Expected Conc. = 0.1264 Report level label = 0.0511 Pct Recovery = 67% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl SpecificMix = 03FF076 Laboratory ID = 20161190075 Lab Value = 0.072 Expected Conc. = 0.1264 Report level label = 0.0511 Pct Recovery = 57% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20173120093 Lab Value = 0.093 Expected Conc. = 0.1023 Report level label = 0.0511 Pct Recovery = 91% Analysis Date = 03/10/18 SpikeMix = ChemService 6472100: 30 µl & ChemService 6537100: 30 µl SpecificMix = 6537100 Laboratory ID = 20172780018 Lab Value = 0.092 Expected Conc. = 0.1023 Report level label = 0.0511 Pct Recovery = 90% Analysis Date = 02/08/18 SpikeMix = ChemService 6537100: 30 µl & Abs 071817Pest: 30 µl SpecificMix = 6537100 Laboratory ID = 20141840097 Lab Value = 0.037 Expected Conc. = 0.1014 Report level label = 0.0511 Pct Recovery = 37% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20141490205 Lab Value = 0.072 Expected Conc. = 0.1014 Report level label = 0.0511 Pct Recovery = 71% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20141420140 Lab Value = 0.068 Expected Conc. = 0.1014 Report level label = 0.0511 Pct Recovery = 67% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20141360094 Lab Value = 0.030 Expected Conc. = 0.1014 Report level label = 0.0511 Pct Recovery = 29% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20133580036 Lab Value = 0.079 Expected Conc. = 0.1 Report level label = 0.0511 Pct Recovery = 79% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 042413 Laboratory ID = 20133190012 Lab Value = 0.087 Expected Conc. = 0.1 Report level label = 0.0511 Pct Recovery = 87% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 042413 Laboratory ID = 20131650073 Lab Value = 0.092 Expected Conc. = 0.1 Report level label = 0.0511 Pct Recovery = 92% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl SpecificMix = 042413 Laboratory ID = 20140730138 Lab Value = 0.035 Expected Conc. = 0.0994 Report level label = 0.0511 Pct Recovery = 35% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 04CC101 Laboratory ID = 20140510043 Lab Value = 0.042 Expected Conc. = 0.0994 Report level label = 0.0511 Pct Recovery = 42% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 04CC101 Laboratory ID = 20133310030 Lab Value = 0.105 Expected Conc. = 0.0994 Report level label = 0.0511 Pct Recovery = 106% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl SpecificMix = 04CC101 Laboratory ID = 20132280016 Lab Value = 0.094 Expected Conc. = 0.0994 Report level label = 0.0511 Pct Recovery = 95% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl SpecificMix = 04CC101 Laboratory ID = 20131510026 Lab Value = 0.093 Expected Conc. = 0.0994 Report level label = 0.0511 Pct Recovery = 94% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl SpecificMix = 04CC101 Laboratory ID = 20152190003 Lab Value = 0.072 Expected Conc. = 0.0766 Report level label = 0.0511 Pct Recovery = 93% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = 0406-15-01 Laboratory ID = 20152040177 Lab Value = 0.039 Expected Conc. = 0.0766 Report level label = 0.0511 Pct Recovery = 50% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl SpecificMix = 0406-15-01 Laboratory ID = 20160430111 Lab Value = 0.058 Expected Conc. = 0.076 Report level label = 0.0511 Pct Recovery = 76% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 3851600 Laboratory ID = 20153030068 Lab Value = 0.050 Expected Conc. = 0.076 Report level label = 0.0511 Pct Recovery = 65% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = 3851600 Laboratory ID = 20151760208 Lab Value = 0.063 Expected Conc. = 0.076 Report level label = 0.0511 Pct Recovery = 83% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl SpecificMix = 3851600 Laboratory ID = 20151380009 Lab Value = 0.065 Expected Conc. = 0.076 Report level label = 0.0511 Pct Recovery = 86% Analysis Date = 05/30/15 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 3851600 Laboratory ID = 20140860102 Lab Value = 0.053 Expected Conc. = 0.0752 Report level label = 0.0511 Pct Recovery = 70% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 012513 Laboratory ID = 20133400002 Lab Value = 0.066 Expected Conc. = 0.0752 Report level label = 0.0511 Pct Recovery = 87% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = 052412 Laboratory ID = 20132910008 Lab Value = 0.034 Expected Conc. = 0.0752 Report level label = 0.0511 Pct Recovery = 46% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = 052412 Laboratory ID = 20131920149 Lab Value = 0.060 Expected Conc. = 0.0752 Report level label = 0.0511 Pct Recovery = 80% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl SpecificMix = 012513 Laboratory ID = 20130650005 Lab Value = 0.050 Expected Conc. = 0.0752 Report level label = 0.0511 Pct Recovery = 66% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl SpecificMix = 052412 Laboratory ID = 20131230084 Lab Value = 0.067 Expected Conc. = 0.0742 Report level label = 0.0511 Pct Recovery = 90% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl SpecificMix = 05BB029 Laboratory ID = 20130510051 Lab Value = 0.058 Expected Conc. = 0.0742 Report level label = 0.0511 Pct Recovery = 78% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl SpecificMix = 05BB029 Analysis Date = 03/09/18 Pct Recovery = 84% Analysis Date = 02/28/18 Pct Recovery = 84% Analysis Date = 02/28/18 Pct Recovery = 84% Analysis Date = 02/19/18 Pct Recovery = 84% Analysis Date = 02/19/18 Pct Recovery = 84% Analysis Date = 02/09/18 Pct Recovery = 83% Analysis Date = 02/09/18 Pct Recovery = 83% Analysis Date = 01/31/18 Pct Recovery = 83% Analysis Date = 01/31/18 Pct Recovery = 83% Analysis Date = 01/22/18 Pct Recovery = 83% Analysis Date = 01/22/18 Pct Recovery = 83% Analysis Date = 01/12/18 Pct Recovery = 83% Analysis Date = 01/12/18 Pct Recovery = 83% Analysis Date = 01/03/18 Pct Recovery = 83% Analysis Date = 01/03/18 Pct Recovery = 83% Analysis Date = 12/24/17 Pct Recovery = 82% Analysis Date = 12/24/17 Pct Recovery = 82% Analysis Date = 12/15/17 Pct Recovery = 82% Analysis Date = 12/15/17 Pct Recovery = 82% Analysis Date = 12/06/17 Pct Recovery = 82% Analysis Date = 12/06/17 Pct Recovery = 82% Analysis Date = 11/26/17 Pct Recovery = 82% Analysis Date = 11/26/17 Pct Recovery = 82% Analysis Date = 11/17/17 Pct Recovery = 81% Analysis Date = 11/17/17 Pct Recovery = 81% Analysis Date = 11/07/17 Pct Recovery = 81% Analysis Date = 11/07/17 Pct Recovery = 81% Analysis Date = 10/29/17 Pct Recovery = 81% Analysis Date = 10/29/17 Pct Recovery = 81% Analysis Date = 10/20/17 Pct Recovery = 81% Analysis Date = 10/20/17 Pct Recovery = 81% Analysis Date = 10/10/17 Pct Recovery = 81% Analysis Date = 10/10/17 Pct Recovery = 81% Analysis Date = 10/01/17 Pct Recovery = 80% Analysis Date = 10/01/17 Pct Recovery = 80% Analysis Date = 09/21/17 Pct Recovery = 80% Analysis Date = 09/21/17 Pct Recovery = 80% Analysis Date = 09/12/17 Pct Recovery = 80% Analysis Date = 09/12/17 Pct Recovery = 80% Analysis Date = 09/03/17 Pct Recovery = 80% Analysis Date = 09/03/17 Pct Recovery = 80% Analysis Date = 08/24/17 Pct Recovery = 80% Analysis Date = 08/24/17 Pct Recovery = 80% Analysis Date = 08/15/17 Pct Recovery = 79% Analysis Date = 08/15/17 Pct Recovery = 79% Analysis Date = 08/06/17 Pct Recovery = 79% Analysis Date = 08/06/17 Pct Recovery = 79% Analysis Date = 07/27/17 Pct Recovery = 79% Analysis Date = 07/27/17 Pct Recovery = 79% Analysis Date = 07/18/17 Pct Recovery = 79% Analysis Date = 07/18/17 Pct Recovery = 79% Analysis Date = 07/08/17 Pct Recovery = 78% Analysis Date = 07/08/17 Pct Recovery = 78% Analysis Date = 06/29/17 Pct Recovery = 78% Analysis Date = 06/29/17 Pct Recovery = 78% Analysis Date = 06/20/17 Pct Recovery = 78% Analysis Date = 06/20/17 Pct Recovery = 78% Analysis Date = 06/10/17 Pct Recovery = 78% Analysis Date = 06/10/17 Pct Recovery = 78% Analysis Date = 06/01/17 Pct Recovery = 78% Analysis Date = 06/01/17 Pct Recovery = 78% Analysis Date = 05/22/17 Pct Recovery = 77% Analysis Date = 05/22/17 Pct Recovery = 77% Analysis Date = 05/13/17 Pct Recovery = 77% Analysis Date = 05/13/17 Pct Recovery = 77% Analysis Date = 05/04/17 Pct Recovery = 77% Analysis Date = 05/04/17 Pct Recovery = 77% Analysis Date = 04/24/17 Pct Recovery = 77% Analysis Date = 04/24/17 Pct Recovery = 77% Analysis Date = 04/15/17 Pct Recovery = 77% Analysis Date = 04/15/17 Pct Recovery = 77% Analysis Date = 04/05/17 Pct Recovery = 76% Analysis Date = 04/05/17 Pct Recovery = 76% Analysis Date = 03/27/17 Pct Recovery = 76% Analysis Date = 03/27/17 Pct Recovery = 76% Analysis Date = 03/18/17 Pct Recovery = 76% Analysis Date = 03/18/17 Pct Recovery = 76% Analysis Date = 03/08/17 Pct Recovery = 76% Analysis Date = 03/08/17 Pct Recovery = 76% Analysis Date = 02/27/17 Pct Recovery = 75% Analysis Date = 02/27/17 Pct Recovery = 75% Analysis Date = 02/18/17 Pct Recovery = 75% Analysis Date = 02/18/17 Pct Recovery = 75% Analysis Date = 02/08/17 Pct Recovery = 75% Analysis Date = 02/08/17 Pct Recovery = 75% Analysis Date = 01/30/17 Pct Recovery = 75% Analysis Date = 01/30/17 Pct Recovery = 75% Analysis Date = 01/20/17 Pct Recovery = 75% Analysis Date = 01/20/17 Pct Recovery = 75% Analysis Date = 01/11/17 Pct Recovery = 74% Analysis Date = 01/11/17 Pct Recovery = 74% Analysis Date = 01/02/17 Pct Recovery = 74% Analysis Date = 01/02/17 Pct Recovery = 74% Analysis Date = 12/23/16 Pct Recovery = 74% Analysis Date = 12/23/16 Pct Recovery = 74% Analysis Date = 12/14/16 Pct Recovery = 74% Analysis Date = 12/14/16 Pct Recovery = 74% Analysis Date = 12/04/16 Pct Recovery = 73% Analysis Date = 12/04/16 Pct Recovery = 73% Analysis Date = 11/25/16 Pct Recovery = 73% Analysis Date = 11/25/16 Pct Recovery = 73% Analysis Date = 11/16/16 Pct Recovery = 73% Analysis Date = 11/16/16 Pct Recovery = 73% Analysis Date = 11/06/16 Pct Recovery = 73% Analysis Date = 11/06/16 Pct Recovery = 73% Analysis Date = 10/28/16 Pct Recovery = 73% Analysis Date = 10/28/16 Pct Recovery = 73% Analysis Date = 10/18/16 Pct Recovery = 72% Analysis Date = 10/18/16 Pct Recovery = 72% Analysis Date = 10/09/16 Pct Recovery = 72% Analysis Date = 10/09/16 Pct Recovery = 72% Analysis Date = 09/30/16 Pct Recovery = 72% Analysis Date = 09/30/16 Pct Recovery = 72% Analysis Date = 09/20/16 Pct Recovery = 72% Analysis Date = 09/20/16 Pct Recovery = 72% Analysis Date = 09/11/16 Pct Recovery = 71% Analysis Date = 09/11/16 Pct Recovery = 71% Analysis Date = 09/01/16 Pct Recovery = 71% Analysis Date = 09/01/16 Pct Recovery = 71% Analysis Date = 08/23/16 Pct Recovery = 71% Analysis Date = 08/23/16 Pct Recovery = 71% Analysis Date = 08/14/16 Pct Recovery = 71% Analysis Date = 08/14/16 Pct Recovery = 71% Analysis Date = 08/04/16 Pct Recovery = 71% Analysis Date = 08/04/16 Pct Recovery = 71% Analysis Date = 07/26/16 Pct Recovery = 70% Analysis Date = 07/26/16 Pct Recovery = 70% Analysis Date = 07/17/16 Pct Recovery = 70% Analysis Date = 07/17/16 Pct Recovery = 70% Analysis Date = 07/07/16 Pct Recovery = 70% Analysis Date = 07/07/16 Pct Recovery = 70% Analysis Date = 06/28/16 Pct Recovery = 70% Analysis Date = 06/28/16 Pct Recovery = 70% Analysis Date = 06/18/16 Pct Recovery = 70% Analysis Date = 06/18/16 Pct Recovery = 70% Analysis Date = 06/09/16 Pct Recovery = 69% Analysis Date = 06/09/16 Pct Recovery = 69% Analysis Date = 05/31/16 Pct Recovery = 69% Analysis Date = 05/31/16 Pct Recovery = 69% Analysis Date = 05/21/16 Pct Recovery = 69% Analysis Date = 05/21/16 Pct Recovery = 69% Analysis Date = 05/12/16 Pct Recovery = 69% Analysis Date = 05/12/16 Pct Recovery = 69% Analysis Date = 05/02/16 Pct Recovery = 68% Analysis Date = 05/02/16 Pct Recovery = 68% Analysis Date = 04/23/16 Pct Recovery = 68% Analysis Date = 04/23/16 Pct Recovery = 68% Analysis Date = 04/14/16 Pct Recovery = 68% Analysis Date = 04/14/16 Pct Recovery = 68% Analysis Date = 04/04/16 Pct Recovery = 68% Analysis Date = 04/04/16 Pct Recovery = 68% Analysis Date = 03/26/16 Pct Recovery = 68% Analysis Date = 03/26/16 Pct Recovery = 68% Analysis Date = 03/16/16 Pct Recovery = 68% Analysis Date = 03/16/16 Pct Recovery = 68% Analysis Date = 03/07/16 Pct Recovery = 67% Analysis Date = 03/07/16 Pct Recovery = 67% Analysis Date = 02/27/16 Pct Recovery = 67% Analysis Date = 02/27/16 Pct Recovery = 67% Analysis Date = 02/17/16 Pct Recovery = 67% Analysis Date = 02/17/16 Pct Recovery = 67% Analysis Date = 02/08/16 Pct Recovery = 67% Analysis Date = 02/08/16 Pct Recovery = 67% Analysis Date = 01/30/16 Pct Recovery = 67% Analysis Date = 01/30/16 Pct Recovery = 67% Analysis Date = 01/20/16 Pct Recovery = 66% Analysis Date = 01/20/16 Pct Recovery = 66% Analysis Date = 01/11/16 Pct Recovery = 66% Analysis Date = 01/11/16 Pct Recovery = 66% Analysis Date = 01/01/16 Pct Recovery = 66% Analysis Date = 01/01/16 Pct Recovery = 66% Analysis Date = 12/23/15 Pct Recovery = 66% Analysis Date = 12/23/15 Pct Recovery = 66% Analysis Date = 12/14/15 Pct Recovery = 66% Analysis Date = 12/14/15 Pct Recovery = 66% Analysis Date = 12/04/15 Pct Recovery = 65% Analysis Date = 12/04/15 Pct Recovery = 65% Analysis Date = 11/25/15 Pct Recovery = 65% Analysis Date = 11/25/15 Pct Recovery = 65% Analysis Date = 11/15/15 Pct Recovery = 65% Analysis Date = 11/15/15 Pct Recovery = 65% Analysis Date = 11/06/15 Pct Recovery = 65% Analysis Date = 11/06/15 Pct Recovery = 65% Analysis Date = 10/28/15 Pct Recovery = 65% Analysis Date = 10/28/15 Pct Recovery = 65% Analysis Date = 10/18/15 Pct Recovery = 64% Analysis Date = 10/18/15 Pct Recovery = 64% Analysis Date = 10/09/15 Pct Recovery = 64% Analysis Date = 10/09/15 Pct Recovery = 64% Analysis Date = 09/29/15 Pct Recovery = 64% Analysis Date = 09/29/15 Pct Recovery = 64% Analysis Date = 09/20/15 Pct Recovery = 64% Analysis Date = 09/20/15 Pct Recovery = 64% Analysis Date = 09/11/15 Pct Recovery = 64% Analysis Date = 09/11/15 Pct Recovery = 64% Analysis Date = 09/01/15 Pct Recovery = 63% Analysis Date = 09/01/15 Pct Recovery = 63% Analysis Date = 08/23/15 Pct Recovery = 63% Analysis Date = 08/23/15 Pct Recovery = 63% Analysis Date = 08/13/15 Pct Recovery = 63% Analysis Date = 08/13/15 Pct Recovery = 63% Analysis Date = 08/04/15 Pct Recovery = 63% Analysis Date = 08/04/15 Pct Recovery = 63% Analysis Date = 07/26/15 Pct Recovery = 63% Analysis Date = 07/26/15 Pct Recovery = 63% Analysis Date = 07/16/15 Pct Recovery = 62% Analysis Date = 07/16/15 Pct Recovery = 62% Analysis Date = 07/07/15 Pct Recovery = 62% Analysis Date = 07/07/15 Pct Recovery = 62% Analysis Date = 06/28/15 Pct Recovery = 62% Analysis Date = 06/28/15 Pct Recovery = 62% Analysis Date = 06/18/15 Pct Recovery = 62% Analysis Date = 06/18/15 Pct Recovery = 62% Analysis Date = 06/09/15 Pct Recovery = 62% Analysis Date = 06/09/15 Pct Recovery = 62% Analysis Date = 05/30/15 Pct Recovery = 61% Analysis Date = 05/30/15 Pct Recovery = 61% Analysis Date = 05/21/15 Pct Recovery = 61% Analysis Date = 05/21/15 Pct Recovery = 61% Analysis Date = 05/12/15 Pct Recovery = 61% Analysis Date = 05/12/15 Pct Recovery = 61% Analysis Date = 05/02/15 Pct Recovery = 61% Analysis Date = 05/02/15 Pct Recovery = 61% Analysis Date = 04/23/15 Pct Recovery = 61% Analysis Date = 04/23/15 Pct Recovery = 61% Analysis Date = 04/13/15 Pct Recovery = 61% Analysis Date = 04/13/15 Pct Recovery = 61% Analysis Date = 04/04/15 Pct Recovery = 61% Analysis Date = 04/04/15 Pct Recovery = 61% Analysis Date = 03/26/15 Pct Recovery = 61% Analysis Date = 03/26/15 Pct Recovery = 61% Analysis Date = 03/16/15 Pct Recovery = 60% Analysis Date = 03/16/15 Pct Recovery = 60% Analysis Date = 03/07/15 Pct Recovery = 60% Analysis Date = 03/07/15 Pct Recovery = 60% Analysis Date = 02/25/15 Pct Recovery = 60% Analysis Date = 02/25/15 Pct Recovery = 60% Analysis Date = 02/16/15 Pct Recovery = 60% Analysis Date = 02/16/15 Pct Recovery = 60% Analysis Date = 02/07/15 Pct Recovery = 60% Analysis Date = 02/07/15 Pct Recovery = 60% Analysis Date = 01/28/15 Pct Recovery = 60% Analysis Date = 01/28/15 Pct Recovery = 60% Analysis Date = 01/19/15 Pct Recovery = 60% Analysis Date = 01/19/15 Pct Recovery = 60% Analysis Date = 01/10/15 Pct Recovery = 60% Analysis Date = 01/10/15 Pct Recovery = 60% Analysis Date = 12/31/14 Pct Recovery = 59% Analysis Date = 12/31/14 Pct Recovery = 59% Analysis Date = 12/22/14 Pct Recovery = 59% Analysis Date = 12/22/14 Pct Recovery = 59% Analysis Date = 12/12/14 Pct Recovery = 59% Analysis Date = 12/12/14 Pct Recovery = 59% Analysis Date = 12/03/14 Pct Recovery = 59% Analysis Date = 12/03/14 Pct Recovery = 59% Analysis Date = 11/24/14 Pct Recovery = 59% Analysis Date = 11/24/14 Pct Recovery = 59% Analysis Date = 11/14/14 Pct Recovery = 59% Analysis Date = 11/14/14 Pct Recovery = 59% Analysis Date = 11/05/14 Pct Recovery = 59% Analysis Date = 11/05/14 Pct Recovery = 59% Analysis Date = 10/26/14 Pct Recovery = 59% Analysis Date = 10/26/14 Pct Recovery = 59% Analysis Date = 10/17/14 Pct Recovery = 58% Analysis Date = 10/17/14 Pct Recovery = 58% Analysis Date = 10/08/14 Pct Recovery = 58% Analysis Date = 10/08/14 Pct Recovery = 58% Analysis Date = 09/28/14 Pct Recovery = 58% Analysis Date = 09/28/14 Pct Recovery = 58% Analysis Date = 09/19/14 Pct Recovery = 58% Analysis Date = 09/19/14 Pct Recovery = 58% Analysis Date = 09/09/14 Pct Recovery = 58% Analysis Date = 09/09/14 Pct Recovery = 58% Analysis Date = 08/31/14 Pct Recovery = 58% Analysis Date = 08/31/14 Pct Recovery = 58% Analysis Date = 08/22/14 Pct Recovery = 58% Analysis Date = 08/22/14 Pct Recovery = 58% Analysis Date = 08/12/14 Pct Recovery = 57% Analysis Date = 08/12/14 Pct Recovery = 57% Analysis Date = 08/03/14 Pct Recovery = 57% Analysis Date = 08/03/14 Pct Recovery = 57% Analysis Date = 07/25/14 Pct Recovery = 57% Analysis Date = 07/25/14 Pct Recovery = 57% Analysis Date = 07/15/14 Pct Recovery = 57% Analysis Date = 07/15/14 Pct Recovery = 57% Analysis Date = 07/06/14 Pct Recovery = 57% Analysis Date = 07/06/14 Pct Recovery = 57% Analysis Date = 06/26/14 Pct Recovery = 57% Analysis Date = 06/26/14 Pct Recovery = 57% Analysis Date = 06/17/14 Pct Recovery = 57% Analysis Date = 06/17/14 Pct Recovery = 57% Analysis Date = 06/08/14 Pct Recovery = 58% Analysis Date = 06/08/14 Pct Recovery = 58% Analysis Date = 05/29/14 Pct Recovery = 58% Analysis Date = 05/29/14 Pct Recovery = 58% Analysis Date = 05/20/14 Pct Recovery = 58% Analysis Date = 05/20/14 Pct Recovery = 58% Analysis Date = 05/10/14 Pct Recovery = 59% Analysis Date = 05/10/14 Pct Recovery = 59% Analysis Date = 05/01/14 Pct Recovery = 59% Analysis Date = 05/01/14 Pct Recovery = 59% Analysis Date = 04/22/14 Pct Recovery = 59% Analysis Date = 04/22/14 Pct Recovery = 59% Analysis Date = 04/12/14 Pct Recovery = 60% Analysis Date = 04/12/14 Pct Recovery = 60% Analysis Date = 04/03/14 Pct Recovery = 60% Analysis Date = 04/03/14 Pct Recovery = 60% Analysis Date = 03/24/14 Pct Recovery = 60% Analysis Date = 03/24/14 Pct Recovery = 60% Analysis Date = 03/15/14 Pct Recovery = 61% Analysis Date = 03/15/14 Pct Recovery = 61% Analysis Date = 03/06/14 Pct Recovery = 61% Analysis Date = 03/06/14 Pct Recovery = 61% Analysis Date = 02/24/14 Pct Recovery = 61% Analysis Date = 02/24/14 Pct Recovery = 61% Analysis Date = 02/15/14 Pct Recovery = 62% Analysis Date = 02/15/14 Pct Recovery = 62% Analysis Date = 02/05/14 Pct Recovery = 63% Analysis Date = 02/05/14 Pct Recovery = 63% Analysis Date = 01/27/14 Pct Recovery = 63% Analysis Date = 01/27/14 Pct Recovery = 63% Analysis Date = 01/18/14 Pct Recovery = 64% Analysis Date = 01/18/14 Pct Recovery = 64% Analysis Date = 01/08/14 Pct Recovery = 64% Analysis Date = 01/08/14 Pct Recovery = 64% Analysis Date = 12/30/13 Pct Recovery = 65% Analysis Date = 12/30/13 Pct Recovery = 65% Analysis Date = 12/21/13 Pct Recovery = 65% Analysis Date = 12/21/13 Pct Recovery = 65% Analysis Date = 12/11/13 Pct Recovery = 66% Analysis Date = 12/11/13 Pct Recovery = 66% Analysis Date = 12/02/13 Pct Recovery = 66% Analysis Date = 12/02/13 Pct Recovery = 66% Analysis Date = 11/22/13 Pct Recovery = 67% Analysis Date = 11/22/13 Pct Recovery = 67% Analysis Date = 11/13/13 Pct Recovery = 67% Analysis Date = 11/13/13 Pct Recovery = 67% Analysis Date = 11/04/13 Pct Recovery = 68% Analysis Date = 11/04/13 Pct Recovery = 68% Analysis Date = 10/25/13 Pct Recovery = 68% Analysis Date = 10/25/13 Pct Recovery = 68% Analysis Date = 10/16/13 Pct Recovery = 69% Analysis Date = 10/16/13 Pct Recovery = 69% Analysis Date = 10/06/13 Pct Recovery = 69% Analysis Date = 10/06/13 Pct Recovery = 69% Analysis Date = 09/27/13 Pct Recovery = 70% Analysis Date = 09/27/13 Pct Recovery = 70% Analysis Date = 09/18/13 Pct Recovery = 70% Analysis Date = 09/18/13 Pct Recovery = 70% Analysis Date = 09/08/13 Pct Recovery = 71% Analysis Date = 09/08/13 Pct Recovery = 71% Analysis Date = 08/30/13 Pct Recovery = 71% Analysis Date = 08/30/13 Pct Recovery = 71% Analysis Date = 08/20/13 Pct Recovery = 72% Analysis Date = 08/20/13 Pct Recovery = 72% Analysis Date = 08/11/13 Pct Recovery = 72% Analysis Date = 08/11/13 Pct Recovery = 72% Analysis Date = 08/02/13 Pct Recovery = 73% Analysis Date = 08/02/13 Pct Recovery = 73% Analysis Date = 07/23/13 Pct Recovery = 73% Analysis Date = 07/23/13 Pct Recovery = 73% Analysis Date = 07/14/13 Pct Recovery = 74% Analysis Date = 07/14/13 Pct Recovery = 74% Analysis Date = 07/05/13 Pct Recovery = 74% Analysis Date = 07/05/13 Pct Recovery = 74% Analysis Date = 06/25/13 Pct Recovery = 75% Analysis Date = 06/25/13 Pct Recovery = 75% Analysis Date = 06/16/13 Pct Recovery = 75% Analysis Date = 06/16/13 Pct Recovery = 75% Analysis Date = 06/06/13 Pct Recovery = 76% Analysis Date = 06/06/13 Pct Recovery = 76% Analysis Date = 05/28/13 Pct Recovery = 76% Analysis Date = 05/28/13 Pct Recovery = 76% Analysis Date = 05/19/13 Pct Recovery = 77% Analysis Date = 05/19/13 Pct Recovery = 77% Analysis Date = 05/09/13 Pct Recovery = 77% Analysis Date = 05/09/13 Pct Recovery = 77% Analysis Date = 04/30/13 Pct Recovery = 78% Analysis Date = 04/30/13 Pct Recovery = 78% Analysis Date = 04/20/13 Pct Recovery = 78% Analysis Date = 04/20/13 Pct Recovery = 78% Analysis Date = 04/11/13 Pct Recovery = 79% Analysis Date = 04/11/13 Pct Recovery = 79% Analysis Date = 04/02/13 Pct Recovery = 79% Analysis Date = 04/02/13 Pct Recovery = 79% Analysis Date = 03/23/13 Pct Recovery = 80% Analysis Date = 03/23/13 Pct Recovery = 80% Analysis Date = 03/14/13 Pct Recovery = 80% Analysis Date = 03/14/13 Pct Recovery = 80% Analysis Date = 03/04/13 Pct Recovery = 81% Analysis Date = 03/04/13 Pct Recovery = 81% Analysis Date = 02/23/13 Pct Recovery = 81% Analysis Date = 02/23/13 Pct Recovery = 81% Analysis Date = 02/14/13 Pct Recovery = 82% Analysis Date = 02/14/13 Pct Recovery = 82% Analysis Date = 02/04/13 Pct Recovery = 82% Analysis Date = 02/04/13 Pct Recovery = 82% Analysis Date = 01/26/13 Pct Recovery = 82% Analysis Date = 01/26/13 Pct Recovery = 82% Analysis Date = 01/17/13 Pct Recovery = 83% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
PHOSMET OXON

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 58 69% 20% 70% 18%
Total 58 69% 20% 70% 18%

Sample Statistics
PHOSMET OXON

Characteristic N % % Basis
Plotted 58 100% Spiked
Estimated Values 58 100% Spiked
Deleted Values 12 10% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 62 .  
False Negatives 0 0% 0 out of 58
Not Spiked 56 .  
False Positives 3 6% 3 out of 48

OBSP Determination:
PROMETON
METHOD: 2033 , TESTIDCODE: 04037GCM35

Laboratory ID = 20132490342 Lab Value = 0.132 Expected Conc. = 0.15 Report level label = 0.012 Pct Recovery = 88% Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20180390003 Lab Value = 0.072 Expected Conc. = 0.08 Report level label = 0.012 Pct Recovery = 90% Analysis Date = 04/06/18 SpikeMix = Spex Organics EN170808006: 100 µl & Abs 071717Pest: 100 µl SpecificMix = 071717Pest Laboratory ID = 20172510330 Lab Value = 0.062 Expected Conc. = 0.08 Report level label = 0.012 Pct Recovery = 77% Analysis Date = 12/29/17 SpikeMix = ChemService 6537100: 100 µl & Abs 071817Pest: 100 µl SpecificMix = 6537100 Laboratory ID = 20132140002 Lab Value = 0.070 Expected Conc. = 0.0752 Report level label = 0.012 Pct Recovery = 93% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl SpecificMix = LB99392 Laboratory ID = 20131370001 Lab Value = 0.083 Expected Conc. = 0.0752 Report level label = 0.012 Pct Recovery = 110% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl SpecificMix = LB99392 Laboratory ID = 20162860079 Lab Value = 0.080 Expected Conc. = 0.075 Report level label = 0.012 Pct Recovery = 106% Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl SpecificMix = 060916 Laboratory ID = 20163150006 Lab Value = 0.069 Expected Conc. = 0.075 Report level label = 0.012 Pct Recovery = 91% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl SpecificMix = 060916 Laboratory ID = 20140370077 Lab Value = 0.045 Expected Conc. = 0.075 Report level label = 0.012 Pct Recovery = 59% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20132560001 Lab Value = 0.073 Expected Conc. = 0.075 Report level label = 0.012 Pct Recovery = 98% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20152610011 Lab Value = 0.053 Expected Conc. = 0.0728 Report level label = 0.012 Pct Recovery = 72% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl SpecificMix = 0406-15-01 Laboratory ID = 20152460215 Lab Value = 0.055 Expected Conc. = 0.0728 Report level label = 0.012 Pct Recovery = 75% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl SpecificMix = 0406-15-01 Laboratory ID = 20171660002 Lab Value = 0.059 Expected Conc. = 0.06 Report level label = 0.012 Pct Recovery = 98% Analysis Date = 08/23/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = 060916 Laboratory ID = 20171380001 Lab Value = 0.043 Expected Conc. = 0.06 Report level label = 0.012 Pct Recovery = 72% Analysis Date = 06/07/17 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 041816 Laboratory ID = 20170740063 Lab Value = 0.057 Expected Conc. = 0.06 Report level label = 0.012 Pct Recovery = 94% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl SpecificMix = 041816 Laboratory ID = 20170190026 Lab Value = 0.057 Expected Conc. = 0.06 Report level label = 0.012 Pct Recovery = 94% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = 060916 Laboratory ID = 20161740258 Lab Value = 0.030 Expected Conc. = 0.06 Report level label = 0.012 Pct Recovery = 50% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 041816 Laboratory ID = 20130940097 Lab Value = 0.039 Expected Conc. = 0.0505 Report level label = 0.012 Pct Recovery = 78% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = 0507-12-04.2 Laboratory ID = 20123560092 Lab Value = 0.036 Expected Conc. = 0.0505 Report level label = 0.012 Pct Recovery = 71% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = 0507-12-04.2 Laboratory ID = 20130810108 Lab Value = 0.041 Expected Conc. = 0.05 Report level label = 0.012 Pct Recovery = 81% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl SpecificMix = LB92783 Laboratory ID = 20130100066 Lab Value = 0.047 Expected Conc. = 0.05 Report level label = 0.012 Pct Recovery = 94% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl SpecificMix = LB92783 Laboratory ID = 20150430092 Lab Value = 0.037 Expected Conc. = 0.048 Report level label = 0.012 Pct Recovery = 77% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl SpecificMix = E1140407002 Laboratory ID = 20143240095 Lab Value = 0.049 Expected Conc. = 0.048 Report level label = 0.012 Pct Recovery = 101% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl SpecificMix = 032714 Laboratory ID = 20143110108 Lab Value = 0.023 Expected Conc. = 0.048 Report level label = 0.012 Pct Recovery = 47% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl SpecificMix = E1140407002 Laboratory ID = 20142720002 Lab Value = 0.032 Expected Conc. = 0.048 Report level label = 0.012 Pct Recovery = 66% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl SpecificMix = E1140407002 Laboratory ID = 20142270001 Lab Value = 0.032 Expected Conc. = 0.048 Report level label = 0.012 Pct Recovery = 67% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl SpecificMix = 032714 Laboratory ID = 20141770149 Lab Value = 0.035 Expected Conc. = 0.048 Report level label = 0.012 Pct Recovery = 73% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl SpecificMix = E1140407002 Laboratory ID = 20141220025 Lab Value = 0.048 Expected Conc. = 0.048 Report level label = 0.012 Pct Recovery = 100% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl SpecificMix = 032714 Laboratory ID = 20173480003 Lab Value = 0.036 Expected Conc. = 0.04 Report level label = 0.012 Pct Recovery = 89% Analysis Date = 04/05/18 SpikeMix = Abs 071717Pest: 50 µl & ChemService 6567600: 50 µl SpecificMix = 071717Pest Laboratory ID = 20172370001 Lab Value = 0.029 Expected Conc. = 0.04 Report level label = 0.012 Pct Recovery = 72% Analysis Date = 11/18/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6537100: 50 µl SpecificMix = 6537100 Laboratory ID = 20172230001 Lab Value = 0.046 Expected Conc. = 0.04 Report level label = 0.012 Pct Recovery = 115% Analysis Date = 10/19/17 SpikeMix = ChemService 6472100: 50 µl & Abs 071717Pest: 50 µl SpecificMix = 071717Pest Laboratory ID = 20160770090 Lab Value = 0.024 Expected Conc. = 0.0364 Report level label = 0.012 Pct Recovery = 67% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20160630046 Lab Value = 0.022 Expected Conc. = 0.0364 Report level label = 0.012 Pct Recovery = 60% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20153510109 Lab Value = 0.023 Expected Conc. = 0.0364 Report level label = 0.012 Pct Recovery = 64% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20153440001 Lab Value = 0.018 Expected Conc. = 0.0364 Report level label = 0.012 Pct Recovery = 49% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20161260151 Lab Value = 0.027 Expected Conc. = 0.036 Report level label = 0.012 Pct Recovery = 74% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = 3851600 Laboratory ID = 20151550293 Lab Value = 0.038 Expected Conc. = 0.036 Report level label = 0.012 Pct Recovery = 106% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl SpecificMix = 3851600 Laboratory ID = 20151270112 Lab Value = 0.027 Expected Conc. = 0.036 Report level label = 0.012 Pct Recovery = 75% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl SpecificMix = 3851600 Laboratory ID = 20172020035 Lab Value = 0.036 Expected Conc. = 0.032 Report level label = 0.012 Pct Recovery = 113% Analysis Date = 11/07/17 SpikeMix = Abs 071717Pest: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 071717Pest Laboratory ID = 20140510043 Lab Value = 0.026 Expected Conc. = 0.0301 Report level label = 0.012 Pct Recovery = 86% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl SpecificMix = LB99392 Laboratory ID = 20133470008 Lab Value = 0.027 Expected Conc. = 0.0301 Report level label = 0.012 Pct Recovery = 90% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl SpecificMix = LB99392 Laboratory ID = 20133190012 Lab Value = 0.029 Expected Conc. = 0.0301 Report level label = 0.012 Pct Recovery = 97% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = LB99392 Laboratory ID = 20133050050 Lab Value = 0.035 Expected Conc. = 0.0301 Report level label = 0.012 Pct Recovery = 117% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl SpecificMix = LB99392 Laboratory ID = 20171940002 Lab Value = 0.028 Expected Conc. = 0.03 Report level label = 0.012 Pct Recovery = 92% Analysis Date = 11/10/17 SpikeMix = ChemService 5054800: 40 µl & NSI 041816: 40 µl SpecificMix = 041816 Laboratory ID = 20171160110 Lab Value = 0.027 Expected Conc. = 0.03 Report level label = 0.012 Pct Recovery = 90% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = 060916 Laboratory ID = 20162520001 Lab Value = 0.036 Expected Conc. = 0.03 Report level label = 0.012 Pct Recovery = 119% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl SpecificMix = 060916 Laboratory ID = 20163560019 Lab Value = 0.024 Expected Conc. = 0.03 Report level label = 0.012 Pct Recovery = 78% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl SpecificMix = 060916 Laboratory ID = 20162380004 Lab Value = 0.028 Expected Conc. = 0.03 Report level label = 0.012 Pct Recovery = 93% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = 060916 Laboratory ID = 20162020124 Lab Value = 0.026 Expected Conc. = 0.03 Report level label = 0.012 Pct Recovery = 85% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl SpecificMix = 041816 Laboratory ID = 20161600087 Lab Value = 0.026 Expected Conc. = 0.03 Report level label = 0.012 Pct Recovery = 87% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 041816 Laboratory ID = 20161340228 Lab Value = 0.022 Expected Conc. = 0.03 Report level label = 0.012 Pct Recovery = 72% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl SpecificMix = 041816 Laboratory ID = 20161190075 Lab Value = 0.020 Expected Conc. = 0.03 Report level label = 0.012 Pct Recovery = 68% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 041816 Laboratory ID = 20133580036 Lab Value = 0.020 Expected Conc. = 0.03 Report level label = 0.012 Pct Recovery = 66% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20131790009 Lab Value = 0.018 Expected Conc. = 0.03 Report level label = 0.012 Pct Recovery = 60% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20131510026 Lab Value = 0.024 Expected Conc. = 0.03 Report level label = 0.012 Pct Recovery = 80% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20180940080 Lab Value = 0.019 Expected Conc. = 0.024 Report level label = 0.012 Pct Recovery = 79% Analysis Date = 05/31/18 SpikeMix = ChemService 6472100: 30 µl & Abs 071717Pest: 30 µl SpecificMix = 071717Pest Laboratory ID = 20180730064 Lab Value = 0.028 Expected Conc. = 0.024 Report level label = 0.012 Pct Recovery = 117% Analysis Date = 05/16/18 SpikeMix = Abs 071717Pest: 30 µl & Abs 071817Pest: 30 µl SpecificMix = 071717Pest Laboratory ID = 20173120093 Lab Value = 0.024 Expected Conc. = 0.024 Report level label = 0.012 Pct Recovery = 102% Analysis Date = 03/10/18 SpikeMix = ChemService 6472100: 30 µl & ChemService 6537100: 30 µl SpecificMix = 6537100 Laboratory ID = 20172780018 Lab Value = 0.017 Expected Conc. = 0.024 Report level label = 0.012 Pct Recovery = 69% Analysis Date = 02/08/18 SpikeMix = ChemService 6537100: 30 µl & Abs 071817Pest: 30 µl SpecificMix = 6537100 Laboratory ID = 20150150115 Lab Value = 0.018 Expected Conc. = 0.024 Report level label = 0.012 Pct Recovery = 74% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl SpecificMix = 032714 Laboratory ID = 20142820151 Lab Value = 0.021 Expected Conc. = 0.024 Report level label = 0.012 Pct Recovery = 88% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl SpecificMix = 032714 Laboratory ID = 20142470041 Lab Value = 0.018 Expected Conc. = 0.024 Report level label = 0.012 Pct Recovery = 76% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141910243 Lab Value = 0.014 Expected Conc. = 0.024 Report level label = 0.012 Pct Recovery = 58% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141640076 Lab Value = 0.019 Expected Conc. = 0.024 Report level label = 0.012 Pct Recovery = 80% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141490205 Lab Value = 0.024 Expected Conc. = 0.024 Report level label = 0.012 Pct Recovery = 100% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = 032714 Laboratory ID = 20141360094 Lab Value = 0.018 Expected Conc. = 0.024 Report level label = 0.012 Pct Recovery = 75% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141080004 Lab Value = 0.020 Expected Conc. = 0.024 Report level label = 0.012 Pct Recovery = 85% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl SpecificMix = 032714 Laboratory ID = 20130510051 Lab Value = 0.016 Expected Conc. = 0.0202 Report level label = 0.012 Pct Recovery = 78% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl SpecificMix = 0507-12-04.2 Laboratory ID = 20130390105 Lab Value = 0.013 Expected Conc. = 0.02 Report level label = 0.012 Pct Recovery = 67% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl SpecificMix = LB92783 Laboratory ID = 20152190003 Lab Value = 0.012 Expected Conc. = 0.0182 Report level label = 0.012 Pct Recovery = 68% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = 0406-15-01 Laboratory ID = 20152040177 Lab Value = 0.016 Expected Conc. = 0.0182 Report level label = 0.012 Pct Recovery = 88% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl SpecificMix = 0406-15-01 Laboratory ID = 20160430111 Lab Value = 0.016 Expected Conc. = 0.018 Report level label = 0.012 Pct Recovery = 90% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 3851600 Laboratory ID = 20160210080 Lab Value = 0.010 Expected Conc. = 0.018 Report level label = 0.012 Pct Recovery = 54% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 3851600 Laboratory ID = 20152950078 Lab Value = 0.010 Expected Conc. = 0.018 Report level label = 0.012 Pct Recovery = 55% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 3851600 Laboratory ID = 20153030068 Lab Value = 0.015 Expected Conc. = 0.018 Report level label = 0.012 Pct Recovery = 83% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = 3851600 Laboratory ID = 20151760208 Lab Value = 0.020 Expected Conc. = 0.018 Report level label = 0.012 Pct Recovery = 110% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl SpecificMix = 3851600 Laboratory ID = 20151380009 Lab Value = 0.013 Expected Conc. = 0.018 Report level label = 0.012 Pct Recovery = 74% Analysis Date = 05/30/15 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 3851600 Analysis Date = 05/31/18 Pct Recovery = 98% Analysis Date = 05/21/18 Pct Recovery = 97% Analysis Date = 05/21/18 Pct Recovery = 97% Analysis Date = 05/11/18 Pct Recovery = 97% Analysis Date = 05/11/18 Pct Recovery = 97% Analysis Date = 05/01/18 Pct Recovery = 97% Analysis Date = 05/01/18 Pct Recovery = 97% Analysis Date = 04/21/18 Pct Recovery = 97% Analysis Date = 04/21/18 Pct Recovery = 97% Analysis Date = 04/11/18 Pct Recovery = 96% Analysis Date = 04/11/18 Pct Recovery = 96% Analysis Date = 04/02/18 Pct Recovery = 96% Analysis Date = 04/02/18 Pct Recovery = 96% Analysis Date = 03/23/18 Pct Recovery = 96% Analysis Date = 03/23/18 Pct Recovery = 96% Analysis Date = 03/13/18 Pct Recovery = 96% Analysis Date = 03/13/18 Pct Recovery = 96% Analysis Date = 03/03/18 Pct Recovery = 95% Analysis Date = 03/03/18 Pct Recovery = 95% Analysis Date = 02/21/18 Pct Recovery = 95% Analysis Date = 02/21/18 Pct Recovery = 95% Analysis Date = 02/12/18 Pct Recovery = 95% Analysis Date = 02/12/18 Pct Recovery = 95% Analysis Date = 02/02/18 Pct Recovery = 95% Analysis Date = 02/02/18 Pct Recovery = 95% Analysis Date = 01/23/18 Pct Recovery = 94% Analysis Date = 01/23/18 Pct Recovery = 94% Analysis Date = 01/13/18 Pct Recovery = 94% Analysis Date = 01/13/18 Pct Recovery = 94% Analysis Date = 01/03/18 Pct Recovery = 94% Analysis Date = 01/03/18 Pct Recovery = 94% Analysis Date = 12/25/17 Pct Recovery = 93% Analysis Date = 12/25/17 Pct Recovery = 93% Analysis Date = 12/15/17 Pct Recovery = 93% Analysis Date = 12/15/17 Pct Recovery = 93% Analysis Date = 12/05/17 Pct Recovery = 93% Analysis Date = 12/05/17 Pct Recovery = 93% Analysis Date = 11/25/17 Pct Recovery = 93% Analysis Date = 11/25/17 Pct Recovery = 93% Analysis Date = 11/15/17 Pct Recovery = 92% Analysis Date = 11/15/17 Pct Recovery = 92% Analysis Date = 11/05/17 Pct Recovery = 92% Analysis Date = 11/05/17 Pct Recovery = 92% Analysis Date = 10/27/17 Pct Recovery = 92% Analysis Date = 10/27/17 Pct Recovery = 92% Analysis Date = 10/17/17 Pct Recovery = 92% Analysis Date = 10/17/17 Pct Recovery = 92% Analysis Date = 10/07/17 Pct Recovery = 91% Analysis Date = 10/07/17 Pct Recovery = 91% Analysis Date = 09/27/17 Pct Recovery = 91% Analysis Date = 09/27/17 Pct Recovery = 91% Analysis Date = 09/17/17 Pct Recovery = 91% Analysis Date = 09/17/17 Pct Recovery = 91% Analysis Date = 09/08/17 Pct Recovery = 91% Analysis Date = 09/08/17 Pct Recovery = 91% Analysis Date = 08/29/17 Pct Recovery = 90% Analysis Date = 08/29/17 Pct Recovery = 90% Analysis Date = 08/19/17 Pct Recovery = 90% Analysis Date = 08/19/17 Pct Recovery = 90% Analysis Date = 08/09/17 Pct Recovery = 90% Analysis Date = 08/09/17 Pct Recovery = 90% Analysis Date = 07/30/17 Pct Recovery = 89% Analysis Date = 07/30/17 Pct Recovery = 89% Analysis Date = 07/21/17 Pct Recovery = 89% Analysis Date = 07/21/17 Pct Recovery = 89% Analysis Date = 07/11/17 Pct Recovery = 89% Analysis Date = 07/11/17 Pct Recovery = 89% Analysis Date = 07/01/17 Pct Recovery = 89% Analysis Date = 07/01/17 Pct Recovery = 89% Analysis Date = 06/21/17 Pct Recovery = 88% Analysis Date = 06/21/17 Pct Recovery = 88% Analysis Date = 06/11/17 Pct Recovery = 88% Analysis Date = 06/11/17 Pct Recovery = 88% Analysis Date = 06/02/17 Pct Recovery = 88% Analysis Date = 06/02/17 Pct Recovery = 88% Analysis Date = 05/23/17 Pct Recovery = 87% Analysis Date = 05/23/17 Pct Recovery = 87% Analysis Date = 05/13/17 Pct Recovery = 87% Analysis Date = 05/13/17 Pct Recovery = 87% Analysis Date = 05/03/17 Pct Recovery = 87% Analysis Date = 05/03/17 Pct Recovery = 87% Analysis Date = 04/23/17 Pct Recovery = 87% Analysis Date = 04/23/17 Pct Recovery = 87% Analysis Date = 04/13/17 Pct Recovery = 86% Analysis Date = 04/13/17 Pct Recovery = 86% Analysis Date = 04/04/17 Pct Recovery = 86% Analysis Date = 04/04/17 Pct Recovery = 86% Analysis Date = 03/25/17 Pct Recovery = 86% Analysis Date = 03/25/17 Pct Recovery = 86% Analysis Date = 03/15/17 Pct Recovery = 85% Analysis Date = 03/15/17 Pct Recovery = 85% Analysis Date = 03/05/17 Pct Recovery = 85% Analysis Date = 03/05/17 Pct Recovery = 85% Analysis Date = 02/23/17 Pct Recovery = 85% Analysis Date = 02/23/17 Pct Recovery = 85% Analysis Date = 02/14/17 Pct Recovery = 85% Analysis Date = 02/14/17 Pct Recovery = 85% Analysis Date = 02/04/17 Pct Recovery = 84% Analysis Date = 02/04/17 Pct Recovery = 84% Analysis Date = 01/25/17 Pct Recovery = 84% Analysis Date = 01/25/17 Pct Recovery = 84% Analysis Date = 01/15/17 Pct Recovery = 84% Analysis Date = 01/15/17 Pct Recovery = 84% Analysis Date = 01/05/17 Pct Recovery = 84% Analysis Date = 01/05/17 Pct Recovery = 84% Analysis Date = 12/27/16 Pct Recovery = 84% Analysis Date = 12/27/16 Pct Recovery = 84% Analysis Date = 12/17/16 Pct Recovery = 83% Analysis Date = 12/17/16 Pct Recovery = 83% Analysis Date = 12/07/16 Pct Recovery = 83% Analysis Date = 12/07/16 Pct Recovery = 83% Analysis Date = 11/27/16 Pct Recovery = 83% Analysis Date = 11/27/16 Pct Recovery = 83% Analysis Date = 11/17/16 Pct Recovery = 83% Analysis Date = 11/17/16 Pct Recovery = 83% Analysis Date = 11/08/16 Pct Recovery = 82% Analysis Date = 11/08/16 Pct Recovery = 82% Analysis Date = 10/29/16 Pct Recovery = 82% Analysis Date = 10/29/16 Pct Recovery = 82% Analysis Date = 10/19/16 Pct Recovery = 82% Analysis Date = 10/19/16 Pct Recovery = 82% Analysis Date = 10/09/16 Pct Recovery = 82% Analysis Date = 10/09/16 Pct Recovery = 82% Analysis Date = 09/29/16 Pct Recovery = 82% Analysis Date = 09/29/16 Pct Recovery = 82% Analysis Date = 09/19/16 Pct Recovery = 81% Analysis Date = 09/19/16 Pct Recovery = 81% Analysis Date = 09/10/16 Pct Recovery = 81% Analysis Date = 09/10/16 Pct Recovery = 81% Analysis Date = 08/31/16 Pct Recovery = 81% Analysis Date = 08/31/16 Pct Recovery = 81% Analysis Date = 08/21/16 Pct Recovery = 81% Analysis Date = 08/21/16 Pct Recovery = 81% Analysis Date = 08/11/16 Pct Recovery = 80% Analysis Date = 08/11/16 Pct Recovery = 80% Analysis Date = 08/01/16 Pct Recovery = 80% Analysis Date = 08/01/16 Pct Recovery = 80% Analysis Date = 07/23/16 Pct Recovery = 80% Analysis Date = 07/23/16 Pct Recovery = 80% Analysis Date = 07/13/16 Pct Recovery = 80% Analysis Date = 07/13/16 Pct Recovery = 80% Analysis Date = 07/03/16 Pct Recovery = 79% Analysis Date = 07/03/16 Pct Recovery = 79% Analysis Date = 06/23/16 Pct Recovery = 79% Analysis Date = 06/23/16 Pct Recovery = 79% Analysis Date = 06/13/16 Pct Recovery = 79% Analysis Date = 06/13/16 Pct Recovery = 79% Analysis Date = 06/04/16 Pct Recovery = 79% Analysis Date = 06/04/16 Pct Recovery = 79% Analysis Date = 05/25/16 Pct Recovery = 79% Analysis Date = 05/25/16 Pct Recovery = 79% Analysis Date = 05/15/16 Pct Recovery = 78% Analysis Date = 05/15/16 Pct Recovery = 78% Analysis Date = 05/05/16 Pct Recovery = 78% Analysis Date = 05/05/16 Pct Recovery = 78% Analysis Date = 04/25/16 Pct Recovery = 78% Analysis Date = 04/25/16 Pct Recovery = 78% Analysis Date = 04/16/16 Pct Recovery = 78% Analysis Date = 04/16/16 Pct Recovery = 78% Analysis Date = 04/06/16 Pct Recovery = 77% Analysis Date = 04/06/16 Pct Recovery = 77% Analysis Date = 03/27/16 Pct Recovery = 77% Analysis Date = 03/27/16 Pct Recovery = 77% Analysis Date = 03/17/16 Pct Recovery = 77% Analysis Date = 03/17/16 Pct Recovery = 77% Analysis Date = 03/07/16 Pct Recovery = 77% Analysis Date = 03/07/16 Pct Recovery = 77% Analysis Date = 02/26/16 Pct Recovery = 77% Analysis Date = 02/26/16 Pct Recovery = 77% Analysis Date = 02/17/16 Pct Recovery = 77% Analysis Date = 02/17/16 Pct Recovery = 77% Analysis Date = 02/07/16 Pct Recovery = 76% Analysis Date = 02/07/16 Pct Recovery = 76% Analysis Date = 01/28/16 Pct Recovery = 76% Analysis Date = 01/28/16 Pct Recovery = 76% Analysis Date = 01/18/16 Pct Recovery = 76% Analysis Date = 01/18/16 Pct Recovery = 76% Analysis Date = 01/08/16 Pct Recovery = 76% Analysis Date = 01/08/16 Pct Recovery = 76% Analysis Date = 12/30/15 Pct Recovery = 76% Analysis Date = 12/30/15 Pct Recovery = 76% Analysis Date = 12/20/15 Pct Recovery = 76% Analysis Date = 12/20/15 Pct Recovery = 76% Analysis Date = 12/10/15 Pct Recovery = 76% Analysis Date = 12/10/15 Pct Recovery = 76% Analysis Date = 11/30/15 Pct Recovery = 76% Analysis Date = 11/30/15 Pct Recovery = 76% Analysis Date = 11/20/15 Pct Recovery = 76% Analysis Date = 11/20/15 Pct Recovery = 76% Analysis Date = 11/11/15 Pct Recovery = 76% Analysis Date = 11/11/15 Pct Recovery = 76% Analysis Date = 11/01/15 Pct Recovery = 76% Analysis Date = 11/01/15 Pct Recovery = 76% Analysis Date = 10/22/15 Pct Recovery = 76% Analysis Date = 10/22/15 Pct Recovery = 76% Analysis Date = 10/12/15 Pct Recovery = 76% Analysis Date = 10/12/15 Pct Recovery = 76% Analysis Date = 10/02/15 Pct Recovery = 76% Analysis Date = 10/02/15 Pct Recovery = 76% Analysis Date = 09/23/15 Pct Recovery = 75% Analysis Date = 09/23/15 Pct Recovery = 75% Analysis Date = 09/13/15 Pct Recovery = 75% Analysis Date = 09/13/15 Pct Recovery = 75% Analysis Date = 09/03/15 Pct Recovery = 75% Analysis Date = 09/03/15 Pct Recovery = 75% Analysis Date = 08/24/15 Pct Recovery = 75% Analysis Date = 08/24/15 Pct Recovery = 75% Analysis Date = 08/14/15 Pct Recovery = 75% Analysis Date = 08/14/15 Pct Recovery = 75% Analysis Date = 08/04/15 Pct Recovery = 75% Analysis Date = 08/04/15 Pct Recovery = 75% Analysis Date = 07/26/15 Pct Recovery = 75% Analysis Date = 07/26/15 Pct Recovery = 75% Analysis Date = 07/16/15 Pct Recovery = 75% Analysis Date = 07/16/15 Pct Recovery = 75% Analysis Date = 07/06/15 Pct Recovery = 76% Analysis Date = 07/06/15 Pct Recovery = 76% Analysis Date = 06/26/15 Pct Recovery = 76% Analysis Date = 06/26/15 Pct Recovery = 76% Analysis Date = 06/16/15 Pct Recovery = 76% Analysis Date = 06/16/15 Pct Recovery = 76% Analysis Date = 06/07/15 Pct Recovery = 76% Analysis Date = 06/07/15 Pct Recovery = 76% Analysis Date = 05/28/15 Pct Recovery = 76% Analysis Date = 05/28/15 Pct Recovery = 76% Analysis Date = 05/18/15 Pct Recovery = 76% Analysis Date = 05/18/15 Pct Recovery = 76% Analysis Date = 05/08/15 Pct Recovery = 77% Analysis Date = 05/08/15 Pct Recovery = 77% Analysis Date = 04/28/15 Pct Recovery = 77% Analysis Date = 04/28/15 Pct Recovery = 77% Analysis Date = 04/19/15 Pct Recovery = 77% Analysis Date = 04/19/15 Pct Recovery = 77% Analysis Date = 04/09/15 Pct Recovery = 77% Analysis Date = 04/09/15 Pct Recovery = 77% Analysis Date = 03/30/15 Pct Recovery = 77% Analysis Date = 03/30/15 Pct Recovery = 77% Analysis Date = 03/20/15 Pct Recovery = 77% Analysis Date = 03/20/15 Pct Recovery = 77% Analysis Date = 03/10/15 Pct Recovery = 78% Analysis Date = 03/10/15 Pct Recovery = 78% Analysis Date = 02/28/15 Pct Recovery = 78% Analysis Date = 02/28/15 Pct Recovery = 78% Analysis Date = 02/19/15 Pct Recovery = 78% Analysis Date = 02/19/15 Pct Recovery = 78% Analysis Date = 02/09/15 Pct Recovery = 78% Analysis Date = 02/09/15 Pct Recovery = 78% Analysis Date = 01/30/15 Pct Recovery = 78% Analysis Date = 01/30/15 Pct Recovery = 78% Analysis Date = 01/20/15 Pct Recovery = 78% Analysis Date = 01/20/15 Pct Recovery = 78% Analysis Date = 01/10/15 Pct Recovery = 79% Analysis Date = 01/10/15 Pct Recovery = 79% Analysis Date = 01/01/15 Pct Recovery = 79% Analysis Date = 01/01/15 Pct Recovery = 79% Analysis Date = 12/22/14 Pct Recovery = 79% Analysis Date = 12/22/14 Pct Recovery = 79% Analysis Date = 12/12/14 Pct Recovery = 79% Analysis Date = 12/12/14 Pct Recovery = 79% Analysis Date = 12/02/14 Pct Recovery = 79% Analysis Date = 12/02/14 Pct Recovery = 79% Analysis Date = 11/22/14 Pct Recovery = 79% Analysis Date = 11/22/14 Pct Recovery = 79% Analysis Date = 11/13/14 Pct Recovery = 80% Analysis Date = 11/13/14 Pct Recovery = 80% Analysis Date = 11/03/14 Pct Recovery = 80% Analysis Date = 11/03/14 Pct Recovery = 80% Analysis Date = 10/24/14 Pct Recovery = 80% Analysis Date = 10/24/14 Pct Recovery = 80% Analysis Date = 10/14/14 Pct Recovery = 80% Analysis Date = 10/14/14 Pct Recovery = 80% Analysis Date = 10/04/14 Pct Recovery = 80% Analysis Date = 10/04/14 Pct Recovery = 80% Analysis Date = 09/25/14 Pct Recovery = 80% Analysis Date = 09/25/14 Pct Recovery = 80% Analysis Date = 09/15/14 Pct Recovery = 80% Analysis Date = 09/15/14 Pct Recovery = 80% Analysis Date = 09/05/14 Pct Recovery = 81% Analysis Date = 09/05/14 Pct Recovery = 81% Analysis Date = 08/26/14 Pct Recovery = 81% Analysis Date = 08/26/14 Pct Recovery = 81% Analysis Date = 08/16/14 Pct Recovery = 81% Analysis Date = 08/16/14 Pct Recovery = 81% Analysis Date = 08/06/14 Pct Recovery = 81% Analysis Date = 08/06/14 Pct Recovery = 81% Analysis Date = 07/28/14 Pct Recovery = 81% Analysis Date = 07/28/14 Pct Recovery = 81% Analysis Date = 07/18/14 Pct Recovery = 81% Analysis Date = 07/18/14 Pct Recovery = 81% Analysis Date = 07/08/14 Pct Recovery = 81% Analysis Date = 07/08/14 Pct Recovery = 81% Analysis Date = 06/28/14 Pct Recovery = 81% Analysis Date = 06/28/14 Pct Recovery = 81% Analysis Date = 06/18/14 Pct Recovery = 81% Analysis Date = 06/18/14 Pct Recovery = 81% Analysis Date = 06/09/14 Pct Recovery = 81% Analysis Date = 06/09/14 Pct Recovery = 81% Analysis Date = 05/30/14 Pct Recovery = 81% Analysis Date = 05/30/14 Pct Recovery = 81% Analysis Date = 05/20/14 Pct Recovery = 81% Analysis Date = 05/20/14 Pct Recovery = 81% Analysis Date = 05/10/14 Pct Recovery = 82% Analysis Date = 05/10/14 Pct Recovery = 82% Analysis Date = 04/30/14 Pct Recovery = 82% Analysis Date = 04/30/14 Pct Recovery = 82% Analysis Date = 04/21/14 Pct Recovery = 82% Analysis Date = 04/21/14 Pct Recovery = 82% Analysis Date = 04/11/14 Pct Recovery = 82% Analysis Date = 04/11/14 Pct Recovery = 82% Analysis Date = 04/01/14 Pct Recovery = 82% Analysis Date = 04/01/14 Pct Recovery = 82% Analysis Date = 03/22/14 Pct Recovery = 82% Analysis Date = 03/22/14 Pct Recovery = 82% Analysis Date = 03/12/14 Pct Recovery = 82% Analysis Date = 03/12/14 Pct Recovery = 82% Analysis Date = 03/03/14 Pct Recovery = 82% Analysis Date = 03/03/14 Pct Recovery = 82% Analysis Date = 02/21/14 Pct Recovery = 82% Analysis Date = 02/21/14 Pct Recovery = 82% Analysis Date = 02/11/14 Pct Recovery = 82% Analysis Date = 02/11/14 Pct Recovery = 82% Analysis Date = 02/01/14 Pct Recovery = 82% Analysis Date = 02/01/14 Pct Recovery = 82% Analysis Date = 01/22/14 Pct Recovery = 82% Analysis Date = 01/22/14 Pct Recovery = 82% Analysis Date = 01/12/14 Pct Recovery = 82% Analysis Date = 01/12/14 Pct Recovery = 82% Analysis Date = 01/03/14 Pct Recovery = 82% Analysis Date = 01/03/14 Pct Recovery = 82% Analysis Date = 12/24/13 Pct Recovery = 82% Analysis Date = 12/24/13 Pct Recovery = 82% Analysis Date = 12/14/13 Pct Recovery = 82% Analysis Date = 12/14/13 Pct Recovery = 82% Analysis Date = 12/04/13 Pct Recovery = 82% Analysis Date = 12/04/13 Pct Recovery = 82% Analysis Date = 11/24/13 Pct Recovery = 83% Analysis Date = 11/24/13 Pct Recovery = 83% Analysis Date = 11/15/13 Pct Recovery = 83% Analysis Date = 11/15/13 Pct Recovery = 83% Analysis Date = 11/05/13 Pct Recovery = 83% Analysis Date = 11/05/13 Pct Recovery = 83% Analysis Date = 10/26/13 Pct Recovery = 83% Analysis Date = 10/26/13 Pct Recovery = 83% Analysis Date = 10/16/13 Pct Recovery = 83% Analysis Date = 10/16/13 Pct Recovery = 83% Analysis Date = 10/06/13 Pct Recovery = 83% Analysis Date = 10/06/13 Pct Recovery = 83% Analysis Date = 09/27/13 Pct Recovery = 83% Analysis Date = 09/27/13 Pct Recovery = 83% Analysis Date = 09/17/13 Pct Recovery = 83% Analysis Date = 09/17/13 Pct Recovery = 83% Analysis Date = 09/07/13 Pct Recovery = 83% Analysis Date = 09/07/13 Pct Recovery = 83% Analysis Date = 08/28/13 Pct Recovery = 83% Analysis Date = 08/28/13 Pct Recovery = 83% Analysis Date = 08/18/13 Pct Recovery = 83% Analysis Date = 08/18/13 Pct Recovery = 83% Analysis Date = 08/09/13 Pct Recovery = 83% Analysis Date = 08/09/13 Pct Recovery = 83% Analysis Date = 07/30/13 Pct Recovery = 83% Analysis Date = 07/30/13 Pct Recovery = 83% Analysis Date = 07/20/13 Pct Recovery = 83% Analysis Date = 07/20/13 Pct Recovery = 83% Analysis Date = 07/10/13 Pct Recovery = 83% Analysis Date = 07/10/13 Pct Recovery = 83% Analysis Date = 06/30/13 Pct Recovery = 83% Analysis Date = 06/30/13 Pct Recovery = 83% Analysis Date = 06/20/13 Pct Recovery = 84% Analysis Date = 06/20/13 Pct Recovery = 84% Analysis Date = 06/11/13 Pct Recovery = 84% Analysis Date = 06/11/13 Pct Recovery = 84% Analysis Date = 06/01/13 Pct Recovery = 84% Analysis Date = 06/01/13 Pct Recovery = 84% Analysis Date = 05/22/13 Pct Recovery = 84% Analysis Date = 05/22/13 Pct Recovery = 84% Analysis Date = 05/12/13 Pct Recovery = 84% Analysis Date = 05/12/13 Pct Recovery = 84% Analysis Date = 05/02/13 Pct Recovery = 84% Analysis Date = 05/02/13 Pct Recovery = 84% Analysis Date = 04/23/13 Pct Recovery = 84% Analysis Date = 04/23/13 Pct Recovery = 84% Analysis Date = 04/13/13 Pct Recovery = 84% Analysis Date = 04/13/13 Pct Recovery = 84% Analysis Date = 04/03/13 Pct Recovery = 84% Analysis Date = 04/03/13 Pct Recovery = 84% Analysis Date = 03/24/13 Pct Recovery = 84% Analysis Date = 03/24/13 Pct Recovery = 84% Analysis Date = 03/14/13 Pct Recovery = 84% Analysis Date = 03/14/13 Pct Recovery = 84% Analysis Date = 03/05/13 Pct Recovery = 84% Analysis Date = 03/05/13 Pct Recovery = 84% Analysis Date = 02/23/13 Pct Recovery = 84% Analysis Date = 02/23/13 Pct Recovery = 84% Analysis Date = 02/13/13 Pct Recovery = 84% Analysis Date = 02/13/13 Pct Recovery = 84% Analysis Date = 02/03/13 Pct Recovery = 84% Analysis Date = 02/03/13 Pct Recovery = 84% Analysis Date = 01/24/13 Pct Recovery = 85% Analysis Date = 01/24/13 Pct Recovery = 85% Analysis Date = 01/15/13 Pct Recovery = 85% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
PROMETON

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 76 82% 17% 80% 16%
Total 76 82% 17% 80% 16%

Sample Statistics
PROMETON

Characteristic N % % Basis
Plotted 76 100% Spiked
Estimated Values 2 3% Spiked
Deleted Values 1 1% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 76 .  
False Negatives 0 0% 0 out of 76
Not Spiked 58 .  
False Positives 0 0% 0 out of 57

OBSP Determination:
PROMETRYN
METHOD: 2033 , TESTIDCODE: 04036GCM39

Laboratory ID = 20130250061 Lab Value = 0.077 Expected Conc. = 0.1 Report level label = 0.01 Pct Recovery = 76% Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl SpecificMix = A088380 Laboratory ID = 20132140002 Lab Value = 0.078 Expected Conc. = 0.0926 Report level label = 0.01 Pct Recovery = 84% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl SpecificMix = LB99392 Laboratory ID = 20131370001 Lab Value = 0.091 Expected Conc. = 0.0926 Report level label = 0.01 Pct Recovery = 99% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl SpecificMix = LB99392 Laboratory ID = 20163370001 Lab Value = 0.053 Expected Conc. = 0.0625 Report level label = 0.01 Pct Recovery = 85% Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl SpecificMix = LC20138V Laboratory ID = 20162860079 Lab Value = 0.065 Expected Conc. = 0.06 Report level label = 0.01 Pct Recovery = 109% Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl SpecificMix = 5054800 Laboratory ID = 20161880109 Lab Value = 0.073 Expected Conc. = 0.06 Report level label = 0.01 Pct Recovery = 122% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl SpecificMix = 5054800 Laboratory ID = 20152750006 Lab Value = 0.009 Expected Conc. = 0.06 Report level label = 0.01 Pct Recovery = 15% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl SpecificMix = 040615 Laboratory ID = 20152610011 Lab Value = 0.032 Expected Conc. = 0.06 Report level label = 0.01 Pct Recovery = 54% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl SpecificMix = 040615 Laboratory ID = 20171720140 Lab Value = 0.048 Expected Conc. = 0.05 Report level label = 0.01 Pct Recovery = 95% Analysis Date = 08/31/17 SpikeMix = Supelco LC20138V: 80 µl & Phenova B20160331: 80 µl SpecificMix = LC20138V Laboratory ID = 20170740063 Lab Value = 0.044 Expected Conc. = 0.05 Report level label = 0.01 Pct Recovery = 89% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl SpecificMix = LC20138V Laboratory ID = 20161470001 Lab Value = 0.047 Expected Conc. = 0.05 Report level label = 0.01 Pct Recovery = 94% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl SpecificMix = LC20138V Laboratory ID = 20140230082 Lab Value = 0.035 Expected Conc. = 0.05 Report level label = 0.01 Pct Recovery = 69% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl SpecificMix = A093651 Laboratory ID = 20132420001 Lab Value = 0.036 Expected Conc. = 0.05 Report level label = 0.01 Pct Recovery = 72% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl SpecificMix = A093651 Laboratory ID = 20130810108 Lab Value = 0.040 Expected Conc. = 0.05 Report level label = 0.01 Pct Recovery = 80% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl SpecificMix = T1120530013 Laboratory ID = 20123560092 Lab Value = 0.037 Expected Conc. = 0.05 Report level label = 0.01 Pct Recovery = 74% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = T1120530013 Laboratory ID = 20171380001 Lab Value = 0.035 Expected Conc. = 0.048 Report level label = 0.01 Pct Recovery = 72% Analysis Date = 06/07/17 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 5054800 Laboratory ID = 20170960001 Lab Value = 0.042 Expected Conc. = 0.048 Report level label = 0.01 Pct Recovery = 88% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl SpecificMix = 5054800 Laboratory ID = 20161740258 Lab Value = 0.033 Expected Conc. = 0.048 Report level label = 0.01 Pct Recovery = 70% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 5054800 Laboratory ID = 20150720069 Lab Value = 0.034 Expected Conc. = 0.0402 Report level label = 0.01 Pct Recovery = 84% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 03DD006 Laboratory ID = 20143110108 Lab Value = 0.028 Expected Conc. = 0.0402 Report level label = 0.01 Pct Recovery = 69% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 03DD006 Laboratory ID = 20142960086 Lab Value = 0.030 Expected Conc. = 0.0402 Report level label = 0.01 Pct Recovery = 75% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 03DD006 Laboratory ID = 20142720002 Lab Value = 0.029 Expected Conc. = 0.0402 Report level label = 0.01 Pct Recovery = 72% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl SpecificMix = LC06435 Laboratory ID = 20142530087 Lab Value = 0.026 Expected Conc. = 0.0402 Report level label = 0.01 Pct Recovery = 65% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl SpecificMix = LC06435 Laboratory ID = 20142270001 Lab Value = 0.028 Expected Conc. = 0.0402 Report level label = 0.01 Pct Recovery = 70% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl SpecificMix = 03DD006 Laboratory ID = 20141570088 Lab Value = 0.037 Expected Conc. = 0.0402 Report level label = 0.01 Pct Recovery = 93% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl SpecificMix = LC06435 Laboratory ID = 20141220025 Lab Value = 0.041 Expected Conc. = 0.0402 Report level label = 0.01 Pct Recovery = 102% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl SpecificMix = LC06435 Laboratory ID = 20140510043 Lab Value = 0.025 Expected Conc. = 0.037 Report level label = 0.01 Pct Recovery = 67% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl SpecificMix = LB99392 Laboratory ID = 20133470008 Lab Value = 0.033 Expected Conc. = 0.037 Report level label = 0.01 Pct Recovery = 90% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl SpecificMix = LB99392 Laboratory ID = 20133190012 Lab Value = 0.036 Expected Conc. = 0.037 Report level label = 0.01 Pct Recovery = 97% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = LB99392 Laboratory ID = 20133050050 Lab Value = 0.031 Expected Conc. = 0.037 Report level label = 0.01 Pct Recovery = 85% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl SpecificMix = LB99392 Laboratory ID = 20172230001 Lab Value = 0.033 Expected Conc. = 0.035 Report level label = 0.01 Pct Recovery = 93% Analysis Date = 10/19/17 SpikeMix = ChemService 6472100: 50 µl & Abs 071717Pest: 50 µl SpecificMix = 6472100 Laboratory ID = 20172560101 Lab Value = 0.024 Expected Conc. = 0.0339 Report level label = 0.01 Pct Recovery = 70% Analysis Date = 12/22/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6567600: 50 µl SpecificMix = EN170808006 Laboratory ID = 20172370001 Lab Value = 0.026 Expected Conc. = 0.0339 Report level label = 0.01 Pct Recovery = 76% Analysis Date = 11/18/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6537100: 50 µl SpecificMix = EN170808006 Laboratory ID = 20161260151 Lab Value = 0.022 Expected Conc. = 0.03 Report level label = 0.01 Pct Recovery = 74% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = EN150513008 Laboratory ID = 20160770090 Lab Value = 0.021 Expected Conc. = 0.03 Report level label = 0.01 Pct Recovery = 68% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = EN150513008 Laboratory ID = 20153510109 Lab Value = 0.020 Expected Conc. = 0.03 Report level label = 0.01 Pct Recovery = 67% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = EN150513008 Laboratory ID = 20152330039 Lab Value = 0.009 Expected Conc. = 0.03 Report level label = 0.01 Pct Recovery = 31% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl SpecificMix = EN150513008 Laboratory ID = 20151900132 Lab Value = 0.008 Expected Conc. = 0.03 Report level label = 0.01 Pct Recovery = 28% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl SpecificMix = 040615 Laboratory ID = 20151550293 Lab Value = 0.020 Expected Conc. = 0.03 Report level label = 0.01 Pct Recovery = 65% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl SpecificMix = 040615 Laboratory ID = 20171510080 Lab Value = 0.023 Expected Conc. = 0.025 Report level label = 0.01 Pct Recovery = 93% Analysis Date = 06/09/17 SpikeMix = Supelco LC20138V: 40 µl & Crescent 03FF076: 40 µl SpecificMix = LC20138V Laboratory ID = 20162520001 Lab Value = 0.025 Expected Conc. = 0.025 Report level label = 0.01 Pct Recovery = 99% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl SpecificMix = LC20138V Laboratory ID = 20162660005 Lab Value = 0.019 Expected Conc. = 0.025 Report level label = 0.01 Pct Recovery = 75% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl SpecificMix = LC20138V Laboratory ID = 20162020124 Lab Value = 0.019 Expected Conc. = 0.025 Report level label = 0.01 Pct Recovery = 78% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl SpecificMix = LC20138V Laboratory ID = 20171940002 Lab Value = 0.022 Expected Conc. = 0.024 Report level label = 0.01 Pct Recovery = 92% Analysis Date = 11/10/17 SpikeMix = ChemService 5054800: 40 µl & NSI 041816: 40 µl SpecificMix = 5054800 Laboratory ID = 20170460061 Lab Value = 0.022 Expected Conc. = 0.024 Report level label = 0.01 Pct Recovery = 90% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl SpecificMix = 5054800 Laboratory ID = 20163560019 Lab Value = 0.020 Expected Conc. = 0.024 Report level label = 0.01 Pct Recovery = 85% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl SpecificMix = 5054800 Laboratory ID = 20162150213 Lab Value = 0.020 Expected Conc. = 0.024 Report level label = 0.01 Pct Recovery = 83% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl SpecificMix = 5054800 Laboratory ID = 20173120093 Lab Value = 0.022 Expected Conc. = 0.021 Report level label = 0.01 Pct Recovery = 104% Analysis Date = 03/10/18 SpikeMix = ChemService 6472100: 30 µl & ChemService 6537100: 30 µl SpecificMix = 6472100 Laboratory ID = 20150150115 Lab Value = 0.015 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 73% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl SpecificMix = LC06435 Laboratory ID = 20143370094 Lab Value = 0.013 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 63% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl SpecificMix = LC06435 Laboratory ID = 20142200164 Lab Value = 0.016 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 80% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 03DD006 Laboratory ID = 20141910243 Lab Value = 0.014 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 69% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = LC06435 Laboratory ID = 20141840097 Lab Value = 0.015 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 76% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl SpecificMix = LC06435 Laboratory ID = 20141640076 Lab Value = 0.017 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 85% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = 03DD006 Laboratory ID = 20141420140 Lab Value = 0.022 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 108% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 03DD006 Laboratory ID = 20141080004 Lab Value = 0.016 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 80% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl SpecificMix = 03DD006 Laboratory ID = 20140860102 Lab Value = 0.014 Expected Conc. = 0.02 Report level label = 0.01 Pct Recovery = 71% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl SpecificMix = A093651 Laboratory ID = 20133400002 Lab Value = 0.017 Expected Conc. = 0.02 Report level label = 0.01 Pct Recovery = 87% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = A093651 Laboratory ID = 20132910008 Lab Value = 0.013 Expected Conc. = 0.02 Report level label = 0.01 Pct Recovery = 66% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = A093651 Laboratory ID = 20131920149 Lab Value = 0.015 Expected Conc. = 0.02 Report level label = 0.01 Pct Recovery = 76% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl SpecificMix = A093651 Laboratory ID = 20131230084 Lab Value = 0.020 Expected Conc. = 0.02 Report level label = 0.01 Pct Recovery = 102% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl SpecificMix = A088380 Laboratory ID = 20130650005 Lab Value = 0.013 Expected Conc. = 0.02 Report level label = 0.01 Pct Recovery = 65% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl SpecificMix = A088380 Laboratory ID = 20130390105 Lab Value = 0.013 Expected Conc. = 0.02 Report level label = 0.01 Pct Recovery = 64% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl SpecificMix = T1120530013 Laboratory ID = 20161050143 Lab Value = 0.013 Expected Conc. = 0.015 Report level label = 0.01 Pct Recovery = 88% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Laboratory ID = 20160430111 Lab Value = 0.013 Expected Conc. = 0.015 Report level label = 0.01 Pct Recovery = 87% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Laboratory ID = 20160560044 Lab Value = 0.012 Expected Conc. = 0.015 Report level label = 0.01 Pct Recovery = 81% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl SpecificMix = EN150513008 Laboratory ID = 20160070059 Lab Value = 0.013 Expected Conc. = 0.015 Report level label = 0.01 Pct Recovery = 89% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = 040615 Laboratory ID = 20153160001 Lab Value = 0.013 Expected Conc. = 0.015 Report level label = 0.01 Pct Recovery = 85% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = EN150513008 Laboratory ID = 20153030068 Lab Value = 0.013 Expected Conc. = 0.015 Report level label = 0.01 Pct Recovery = 85% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150513008 Laboratory ID = 20152190003 Lab Value = 0.003 Expected Conc. = 0.015 Report level label = 0.01 Pct Recovery = 19% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150513008 Laboratory ID = 20151480170 Lab Value = 0.012 Expected Conc. = 0.015 Report level label = 0.01 Pct Recovery = 80% Analysis Date = 06/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150513008 Laboratory ID = 20151380009 Lab Value = 0.011 Expected Conc. = 0.015 Report level label = 0.01 Pct Recovery = 76% Analysis Date = 05/30/15 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Laboratory ID = 20151210037 Lab Value = 0.014 Expected Conc. = 0.015 Report level label = 0.01 Pct Recovery = 91% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Analysis Date = 03/10/18 Pct Recovery = 96% Analysis Date = 02/28/18 Pct Recovery = 95% Analysis Date = 02/28/18 Pct Recovery = 95% Analysis Date = 02/19/18 Pct Recovery = 95% Analysis Date = 02/19/18 Pct Recovery = 95% Analysis Date = 02/09/18 Pct Recovery = 95% Analysis Date = 02/09/18 Pct Recovery = 95% Analysis Date = 01/31/18 Pct Recovery = 95% Analysis Date = 01/31/18 Pct Recovery = 95% Analysis Date = 01/22/18 Pct Recovery = 95% Analysis Date = 01/22/18 Pct Recovery = 95% Analysis Date = 01/12/18 Pct Recovery = 94% Analysis Date = 01/12/18 Pct Recovery = 94% Analysis Date = 01/03/18 Pct Recovery = 94% Analysis Date = 01/03/18 Pct Recovery = 94% Analysis Date = 12/24/17 Pct Recovery = 94% Analysis Date = 12/24/17 Pct Recovery = 94% Analysis Date = 12/15/17 Pct Recovery = 94% Analysis Date = 12/15/17 Pct Recovery = 94% Analysis Date = 12/06/17 Pct Recovery = 93% Analysis Date = 12/06/17 Pct Recovery = 93% Analysis Date = 11/26/17 Pct Recovery = 93% Analysis Date = 11/26/17 Pct Recovery = 93% Analysis Date = 11/17/17 Pct Recovery = 93% Analysis Date = 11/17/17 Pct Recovery = 93% Analysis Date = 11/07/17 Pct Recovery = 93% Analysis Date = 11/07/17 Pct Recovery = 93% Analysis Date = 10/29/17 Pct Recovery = 93% Analysis Date = 10/29/17 Pct Recovery = 93% Analysis Date = 10/20/17 Pct Recovery = 92% Analysis Date = 10/20/17 Pct Recovery = 92% Analysis Date = 10/10/17 Pct Recovery = 92% Analysis Date = 10/10/17 Pct Recovery = 92% Analysis Date = 10/01/17 Pct Recovery = 92% Analysis Date = 10/01/17 Pct Recovery = 92% Analysis Date = 09/21/17 Pct Recovery = 91% Analysis Date = 09/21/17 Pct Recovery = 91% Analysis Date = 09/12/17 Pct Recovery = 91% Analysis Date = 09/12/17 Pct Recovery = 91% Analysis Date = 09/03/17 Pct Recovery = 91% Analysis Date = 09/03/17 Pct Recovery = 91% Analysis Date = 08/24/17 Pct Recovery = 91% Analysis Date = 08/24/17 Pct Recovery = 91% Analysis Date = 08/15/17 Pct Recovery = 90% Analysis Date = 08/15/17 Pct Recovery = 90% Analysis Date = 08/05/17 Pct Recovery = 90% Analysis Date = 08/05/17 Pct Recovery = 90% Analysis Date = 07/27/17 Pct Recovery = 90% Analysis Date = 07/27/17 Pct Recovery = 90% Analysis Date = 07/18/17 Pct Recovery = 90% Analysis Date = 07/18/17 Pct Recovery = 90% Analysis Date = 07/08/17 Pct Recovery = 89% Analysis Date = 07/08/17 Pct Recovery = 89% Analysis Date = 06/29/17 Pct Recovery = 89% Analysis Date = 06/29/17 Pct Recovery = 89% Analysis Date = 06/19/17 Pct Recovery = 89% Analysis Date = 06/19/17 Pct Recovery = 89% Analysis Date = 06/10/17 Pct Recovery = 89% Analysis Date = 06/10/17 Pct Recovery = 89% Analysis Date = 06/01/17 Pct Recovery = 88% Analysis Date = 06/01/17 Pct Recovery = 88% Analysis Date = 05/22/17 Pct Recovery = 88% Analysis Date = 05/22/17 Pct Recovery = 88% Analysis Date = 05/13/17 Pct Recovery = 88% Analysis Date = 05/13/17 Pct Recovery = 88% Analysis Date = 05/03/17 Pct Recovery = 88% Analysis Date = 05/03/17 Pct Recovery = 88% Analysis Date = 04/24/17 Pct Recovery = 87% Analysis Date = 04/24/17 Pct Recovery = 87% Analysis Date = 04/15/17 Pct Recovery = 87% Analysis Date = 04/15/17 Pct Recovery = 87% Analysis Date = 04/05/17 Pct Recovery = 87% Analysis Date = 04/05/17 Pct Recovery = 87% Analysis Date = 03/27/17 Pct Recovery = 86% Analysis Date = 03/27/17 Pct Recovery = 86% Analysis Date = 03/17/17 Pct Recovery = 86% Analysis Date = 03/17/17 Pct Recovery = 86% Analysis Date = 03/08/17 Pct Recovery = 86% Analysis Date = 03/08/17 Pct Recovery = 86% Analysis Date = 02/27/17 Pct Recovery = 86% Analysis Date = 02/27/17 Pct Recovery = 86% Analysis Date = 02/17/17 Pct Recovery = 85% Analysis Date = 02/17/17 Pct Recovery = 85% Analysis Date = 02/08/17 Pct Recovery = 85% Analysis Date = 02/08/17 Pct Recovery = 85% Analysis Date = 01/29/17 Pct Recovery = 85% Analysis Date = 01/29/17 Pct Recovery = 85% Analysis Date = 01/20/17 Pct Recovery = 84% Analysis Date = 01/20/17 Pct Recovery = 84% Analysis Date = 01/11/17 Pct Recovery = 84% Analysis Date = 01/11/17 Pct Recovery = 84% Analysis Date = 01/01/17 Pct Recovery = 84% Analysis Date = 01/01/17 Pct Recovery = 84% Analysis Date = 12/23/16 Pct Recovery = 83% Analysis Date = 12/23/16 Pct Recovery = 83% Analysis Date = 12/13/16 Pct Recovery = 83% Analysis Date = 12/13/16 Pct Recovery = 83% Analysis Date = 12/04/16 Pct Recovery = 83% Analysis Date = 12/04/16 Pct Recovery = 83% Analysis Date = 11/25/16 Pct Recovery = 83% Analysis Date = 11/25/16 Pct Recovery = 83% Analysis Date = 11/15/16 Pct Recovery = 82% Analysis Date = 11/15/16 Pct Recovery = 82% Analysis Date = 11/06/16 Pct Recovery = 82% Analysis Date = 11/06/16 Pct Recovery = 82% Analysis Date = 10/27/16 Pct Recovery = 82% Analysis Date = 10/27/16 Pct Recovery = 82% Analysis Date = 10/18/16 Pct Recovery = 81% Analysis Date = 10/18/16 Pct Recovery = 81% Analysis Date = 10/09/16 Pct Recovery = 81% Analysis Date = 10/09/16 Pct Recovery = 81% Analysis Date = 09/29/16 Pct Recovery = 81% Analysis Date = 09/29/16 Pct Recovery = 81% Analysis Date = 09/20/16 Pct Recovery = 80% Analysis Date = 09/20/16 Pct Recovery = 80% Analysis Date = 09/10/16 Pct Recovery = 80% Analysis Date = 09/10/16 Pct Recovery = 80% Analysis Date = 09/01/16 Pct Recovery = 80% Analysis Date = 09/01/16 Pct Recovery = 80% Analysis Date = 08/23/16 Pct Recovery = 79% Analysis Date = 08/23/16 Pct Recovery = 79% Analysis Date = 08/13/16 Pct Recovery = 79% Analysis Date = 08/13/16 Pct Recovery = 79% Analysis Date = 08/04/16 Pct Recovery = 79% Analysis Date = 08/04/16 Pct Recovery = 79% Analysis Date = 07/25/16 Pct Recovery = 78% Analysis Date = 07/25/16 Pct Recovery = 78% Analysis Date = 07/16/16 Pct Recovery = 78% Analysis Date = 07/16/16 Pct Recovery = 78% Analysis Date = 07/07/16 Pct Recovery = 78% Analysis Date = 07/07/16 Pct Recovery = 78% Analysis Date = 06/27/16 Pct Recovery = 77% Analysis Date = 06/27/16 Pct Recovery = 77% Analysis Date = 06/18/16 Pct Recovery = 77% Analysis Date = 06/18/16 Pct Recovery = 77% Analysis Date = 06/08/16 Pct Recovery = 77% Analysis Date = 06/08/16 Pct Recovery = 77% Analysis Date = 05/30/16 Pct Recovery = 76% Analysis Date = 05/30/16 Pct Recovery = 76% Analysis Date = 05/21/16 Pct Recovery = 76% Analysis Date = 05/21/16 Pct Recovery = 76% Analysis Date = 05/11/16 Pct Recovery = 75% Analysis Date = 05/11/16 Pct Recovery = 75% Analysis Date = 05/02/16 Pct Recovery = 75% Analysis Date = 05/02/16 Pct Recovery = 75% Analysis Date = 04/22/16 Pct Recovery = 75% Analysis Date = 04/22/16 Pct Recovery = 75% Analysis Date = 04/13/16 Pct Recovery = 74% Analysis Date = 04/13/16 Pct Recovery = 74% Analysis Date = 04/04/16 Pct Recovery = 74% Analysis Date = 04/04/16 Pct Recovery = 74% Analysis Date = 03/25/16 Pct Recovery = 74% Analysis Date = 03/25/16 Pct Recovery = 74% Analysis Date = 03/16/16 Pct Recovery = 73% Analysis Date = 03/16/16 Pct Recovery = 73% Analysis Date = 03/06/16 Pct Recovery = 73% Analysis Date = 03/06/16 Pct Recovery = 73% Analysis Date = 02/26/16 Pct Recovery = 73% Analysis Date = 02/26/16 Pct Recovery = 73% Analysis Date = 02/17/16 Pct Recovery = 72% Analysis Date = 02/17/16 Pct Recovery = 72% Analysis Date = 02/07/16 Pct Recovery = 72% Analysis Date = 02/07/16 Pct Recovery = 72% Analysis Date = 01/29/16 Pct Recovery = 72% Analysis Date = 01/29/16 Pct Recovery = 72% Analysis Date = 01/19/16 Pct Recovery = 71% Analysis Date = 01/19/16 Pct Recovery = 71% Analysis Date = 01/10/16 Pct Recovery = 71% Analysis Date = 01/10/16 Pct Recovery = 71% Analysis Date = 01/01/16 Pct Recovery = 71% Analysis Date = 01/01/16 Pct Recovery = 71% Analysis Date = 12/22/15 Pct Recovery = 71% Analysis Date = 12/22/15 Pct Recovery = 71% Analysis Date = 12/13/15 Pct Recovery = 70% Analysis Date = 12/13/15 Pct Recovery = 70% Analysis Date = 12/03/15 Pct Recovery = 70% Analysis Date = 12/03/15 Pct Recovery = 70% Analysis Date = 11/24/15 Pct Recovery = 70% Analysis Date = 11/24/15 Pct Recovery = 70% Analysis Date = 11/15/15 Pct Recovery = 70% Analysis Date = 11/15/15 Pct Recovery = 70% Analysis Date = 11/05/15 Pct Recovery = 69% Analysis Date = 11/05/15 Pct Recovery = 69% Analysis Date = 10/27/15 Pct Recovery = 69% Analysis Date = 10/27/15 Pct Recovery = 69% Analysis Date = 10/17/15 Pct Recovery = 69% Analysis Date = 10/17/15 Pct Recovery = 69% Analysis Date = 10/08/15 Pct Recovery = 69% Analysis Date = 10/08/15 Pct Recovery = 69% Analysis Date = 09/29/15 Pct Recovery = 68% Analysis Date = 09/29/15 Pct Recovery = 68% Analysis Date = 09/19/15 Pct Recovery = 68% Analysis Date = 09/19/15 Pct Recovery = 68% Analysis Date = 09/10/15 Pct Recovery = 68% Analysis Date = 09/10/15 Pct Recovery = 68% Analysis Date = 08/31/15 Pct Recovery = 68% Analysis Date = 08/31/15 Pct Recovery = 68% Analysis Date = 08/22/15 Pct Recovery = 68% Analysis Date = 08/22/15 Pct Recovery = 68% Analysis Date = 08/13/15 Pct Recovery = 68% Analysis Date = 08/13/15 Pct Recovery = 68% Analysis Date = 08/03/15 Pct Recovery = 68% Analysis Date = 08/03/15 Pct Recovery = 68% Analysis Date = 07/25/15 Pct Recovery = 68% Analysis Date = 07/25/15 Pct Recovery = 68% Analysis Date = 07/15/15 Pct Recovery = 68% Analysis Date = 07/15/15 Pct Recovery = 68% Analysis Date = 07/06/15 Pct Recovery = 68% Analysis Date = 07/06/15 Pct Recovery = 68% Analysis Date = 06/27/15 Pct Recovery = 68% Analysis Date = 06/27/15 Pct Recovery = 68% Analysis Date = 06/17/15 Pct Recovery = 68% Analysis Date = 06/17/15 Pct Recovery = 68% Analysis Date = 06/08/15 Pct Recovery = 68% Analysis Date = 06/08/15 Pct Recovery = 68% Analysis Date = 05/29/15 Pct Recovery = 68% Analysis Date = 05/29/15 Pct Recovery = 68% Analysis Date = 05/20/15 Pct Recovery = 68% Analysis Date = 05/20/15 Pct Recovery = 68% Analysis Date = 05/11/15 Pct Recovery = 68% Analysis Date = 05/11/15 Pct Recovery = 68% Analysis Date = 05/01/15 Pct Recovery = 68% Analysis Date = 05/01/15 Pct Recovery = 68% Analysis Date = 04/22/15 Pct Recovery = 68% Analysis Date = 04/22/15 Pct Recovery = 68% Analysis Date = 04/12/15 Pct Recovery = 69% Analysis Date = 04/12/15 Pct Recovery = 69% Analysis Date = 04/03/15 Pct Recovery = 69% Analysis Date = 04/03/15 Pct Recovery = 69% Analysis Date = 03/25/15 Pct Recovery = 69% Analysis Date = 03/25/15 Pct Recovery = 69% Analysis Date = 03/15/15 Pct Recovery = 69% Analysis Date = 03/15/15 Pct Recovery = 69% Analysis Date = 03/06/15 Pct Recovery = 69% Analysis Date = 03/06/15 Pct Recovery = 69% Analysis Date = 02/24/15 Pct Recovery = 69% Analysis Date = 02/24/15 Pct Recovery = 69% Analysis Date = 02/15/15 Pct Recovery = 69% Analysis Date = 02/15/15 Pct Recovery = 69% Analysis Date = 02/06/15 Pct Recovery = 69% Analysis Date = 02/06/15 Pct Recovery = 69% Analysis Date = 01/27/15 Pct Recovery = 70% Analysis Date = 01/27/15 Pct Recovery = 70% Analysis Date = 01/18/15 Pct Recovery = 70% Analysis Date = 01/18/15 Pct Recovery = 70% Analysis Date = 01/08/15 Pct Recovery = 70% Analysis Date = 01/08/15 Pct Recovery = 70% Analysis Date = 12/30/14 Pct Recovery = 71% Analysis Date = 12/30/14 Pct Recovery = 71% Analysis Date = 12/21/14 Pct Recovery = 71% Analysis Date = 12/21/14 Pct Recovery = 71% Analysis Date = 12/11/14 Pct Recovery = 71% Analysis Date = 12/11/14 Pct Recovery = 71% Analysis Date = 12/02/14 Pct Recovery = 72% Analysis Date = 12/02/14 Pct Recovery = 72% Analysis Date = 11/22/14 Pct Recovery = 72% Analysis Date = 11/22/14 Pct Recovery = 72% Analysis Date = 11/13/14 Pct Recovery = 73% Analysis Date = 11/13/14 Pct Recovery = 73% Analysis Date = 11/04/14 Pct Recovery = 73% Analysis Date = 11/04/14 Pct Recovery = 73% Analysis Date = 10/25/14 Pct Recovery = 73% Analysis Date = 10/25/14 Pct Recovery = 73% Analysis Date = 10/16/14 Pct Recovery = 74% Analysis Date = 10/16/14 Pct Recovery = 74% Analysis Date = 10/06/14 Pct Recovery = 74% Analysis Date = 10/06/14 Pct Recovery = 74% Analysis Date = 09/27/14 Pct Recovery = 74% Analysis Date = 09/27/14 Pct Recovery = 74% Analysis Date = 09/18/14 Pct Recovery = 75% Analysis Date = 09/18/14 Pct Recovery = 75% Analysis Date = 09/08/14 Pct Recovery = 75% Analysis Date = 09/08/14 Pct Recovery = 75% Analysis Date = 08/30/14 Pct Recovery = 76% Analysis Date = 08/30/14 Pct Recovery = 76% Analysis Date = 08/20/14 Pct Recovery = 76% Analysis Date = 08/20/14 Pct Recovery = 76% Analysis Date = 08/11/14 Pct Recovery = 76% Analysis Date = 08/11/14 Pct Recovery = 76% Analysis Date = 08/02/14 Pct Recovery = 77% Analysis Date = 08/02/14 Pct Recovery = 77% Analysis Date = 07/23/14 Pct Recovery = 77% Analysis Date = 07/23/14 Pct Recovery = 77% Analysis Date = 07/14/14 Pct Recovery = 77% Analysis Date = 07/14/14 Pct Recovery = 77% Analysis Date = 07/04/14 Pct Recovery = 77% Analysis Date = 07/04/14 Pct Recovery = 77% Analysis Date = 06/25/14 Pct Recovery = 78% Analysis Date = 06/25/14 Pct Recovery = 78% Analysis Date = 06/16/14 Pct Recovery = 78% Analysis Date = 06/16/14 Pct Recovery = 78% Analysis Date = 06/06/14 Pct Recovery = 78% Analysis Date = 06/06/14 Pct Recovery = 78% Analysis Date = 05/28/14 Pct Recovery = 78% Analysis Date = 05/28/14 Pct Recovery = 78% Analysis Date = 05/18/14 Pct Recovery = 78% Analysis Date = 05/18/14 Pct Recovery = 78% Analysis Date = 05/09/14 Pct Recovery = 78% Analysis Date = 05/09/14 Pct Recovery = 78% Analysis Date = 04/30/14 Pct Recovery = 78% Analysis Date = 04/30/14 Pct Recovery = 78% Analysis Date = 04/20/14 Pct Recovery = 79% Analysis Date = 04/20/14 Pct Recovery = 79% Analysis Date = 04/11/14 Pct Recovery = 79% Analysis Date = 04/11/14 Pct Recovery = 79% Analysis Date = 04/01/14 Pct Recovery = 79% Analysis Date = 04/01/14 Pct Recovery = 79% Analysis Date = 03/23/14 Pct Recovery = 79% Analysis Date = 03/23/14 Pct Recovery = 79% Analysis Date = 03/14/14 Pct Recovery = 79% Analysis Date = 03/14/14 Pct Recovery = 79% Analysis Date = 03/04/14 Pct Recovery = 79% Analysis Date = 03/04/14 Pct Recovery = 79% Analysis Date = 02/23/14 Pct Recovery = 79% Analysis Date = 02/23/14 Pct Recovery = 79% Analysis Date = 02/13/14 Pct Recovery = 79% Analysis Date = 02/13/14 Pct Recovery = 79% Analysis Date = 02/04/14 Pct Recovery = 79% Analysis Date = 02/04/14 Pct Recovery = 79% Analysis Date = 01/26/14 Pct Recovery = 79% Analysis Date = 01/26/14 Pct Recovery = 79% Analysis Date = 01/16/14 Pct Recovery = 79% Analysis Date = 01/16/14 Pct Recovery = 79% Analysis Date = 01/07/14 Pct Recovery = 79% Analysis Date = 01/07/14 Pct Recovery = 79% Analysis Date = 12/28/13 Pct Recovery = 79% Analysis Date = 12/28/13 Pct Recovery = 79% Analysis Date = 12/19/13 Pct Recovery = 80% Analysis Date = 12/19/13 Pct Recovery = 80% Analysis Date = 12/10/13 Pct Recovery = 80% Analysis Date = 12/10/13 Pct Recovery = 80% Analysis Date = 11/30/13 Pct Recovery = 80% Analysis Date = 11/30/13 Pct Recovery = 80% Analysis Date = 11/21/13 Pct Recovery = 80% Analysis Date = 11/21/13 Pct Recovery = 80% Analysis Date = 11/11/13 Pct Recovery = 80% Analysis Date = 11/11/13 Pct Recovery = 80% Analysis Date = 11/02/13 Pct Recovery = 80% Analysis Date = 11/02/13 Pct Recovery = 80% Analysis Date = 10/24/13 Pct Recovery = 80% Analysis Date = 10/24/13 Pct Recovery = 80% Analysis Date = 10/14/13 Pct Recovery = 80% Analysis Date = 10/14/13 Pct Recovery = 80% Analysis Date = 10/05/13 Pct Recovery = 80% Analysis Date = 10/05/13 Pct Recovery = 80% Analysis Date = 09/25/13 Pct Recovery = 80% Analysis Date = 09/25/13 Pct Recovery = 80% Analysis Date = 09/16/13 Pct Recovery = 80% Analysis Date = 09/16/13 Pct Recovery = 80% Analysis Date = 09/07/13 Pct Recovery = 80% Analysis Date = 09/07/13 Pct Recovery = 80% Analysis Date = 08/28/13 Pct Recovery = 80% Analysis Date = 08/28/13 Pct Recovery = 80% Analysis Date = 08/19/13 Pct Recovery = 80% Analysis Date = 08/19/13 Pct Recovery = 80% Analysis Date = 08/09/13 Pct Recovery = 80% Analysis Date = 08/09/13 Pct Recovery = 80% Analysis Date = 07/31/13 Pct Recovery = 80% Analysis Date = 07/31/13 Pct Recovery = 80% Analysis Date = 07/22/13 Pct Recovery = 80% Analysis Date = 07/22/13 Pct Recovery = 80% Analysis Date = 07/12/13 Pct Recovery = 80% Analysis Date = 07/12/13 Pct Recovery = 80% Analysis Date = 07/03/13 Pct Recovery = 80% Analysis Date = 07/03/13 Pct Recovery = 80% Analysis Date = 06/23/13 Pct Recovery = 80% Analysis Date = 06/23/13 Pct Recovery = 80% Analysis Date = 06/14/13 Pct Recovery = 80% Analysis Date = 06/14/13 Pct Recovery = 80% Analysis Date = 06/05/13 Pct Recovery = 80% Analysis Date = 06/05/13 Pct Recovery = 80% Analysis Date = 05/26/13 Pct Recovery = 81% Analysis Date = 05/26/13 Pct Recovery = 81% Analysis Date = 05/17/13 Pct Recovery = 81% Analysis Date = 05/17/13 Pct Recovery = 81% Analysis Date = 05/07/13 Pct Recovery = 81% Analysis Date = 05/07/13 Pct Recovery = 81% Analysis Date = 04/28/13 Pct Recovery = 81% Analysis Date = 04/28/13 Pct Recovery = 81% Analysis Date = 04/19/13 Pct Recovery = 81% Analysis Date = 04/19/13 Pct Recovery = 81% Analysis Date = 04/09/13 Pct Recovery = 81% Analysis Date = 04/09/13 Pct Recovery = 81% Analysis Date = 03/31/13 Pct Recovery = 81% Analysis Date = 03/31/13 Pct Recovery = 81% Analysis Date = 03/21/13 Pct Recovery = 81% Analysis Date = 03/21/13 Pct Recovery = 81% Analysis Date = 03/12/13 Pct Recovery = 81% Analysis Date = 03/12/13 Pct Recovery = 81% Analysis Date = 03/03/13 Pct Recovery = 81% Analysis Date = 03/03/13 Pct Recovery = 81% Analysis Date = 02/21/13 Pct Recovery = 81% Analysis Date = 02/21/13 Pct Recovery = 81% Analysis Date = 02/12/13 Pct Recovery = 81% Analysis Date = 02/12/13 Pct Recovery = 81% Analysis Date = 02/02/13 Pct Recovery = 81% Analysis Date = 02/02/13 Pct Recovery = 81% Analysis Date = 01/24/13 Pct Recovery = 81% Analysis Date = 01/24/13 Pct Recovery = 81% Analysis Date = 01/15/13 Pct Recovery = 81% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
PROMETRYN

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 73 78% 18% 80% 14%
Total 73 78% 18% 80% 14%

Sample Statistics
PROMETRYN

Characteristic N % % Basis
Plotted 73 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 73 .  
False Negatives 0 0% 0 out of 73
Not Spiked 39 .  
False Positives 1 3% 1 out of 39

OBSP Determination:
PROPANIL
METHOD: 2033 , TESTIDCODE: 82679GCM35

Laboratory ID = 20132490342 Lab Value = 0.161 Expected Conc. = 0.199 Report level label = 0.01 Pct Recovery = 81% Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20132140002 Lab Value = 0.080 Expected Conc. = 0.1 Report level label = 0.01 Pct Recovery = 80% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl SpecificMix = LB99392 Laboratory ID = 20131370001 Lab Value = 0.113 Expected Conc. = 0.1 Report level label = 0.01 Pct Recovery = 113% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl SpecificMix = LB99392 Laboratory ID = 20140370077 Lab Value = 0.076 Expected Conc. = 0.0995 Report level label = 0.01 Pct Recovery = 76% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20132560001 Lab Value = 0.081 Expected Conc. = 0.0995 Report level label = 0.01 Pct Recovery = 81% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20130940097 Lab Value = 0.069 Expected Conc. = 0.075 Report level label = 0.01 Pct Recovery = 92% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = 0507-12-04.2 Laboratory ID = 20130810108 Lab Value = 0.079 Expected Conc. = 0.075 Report level label = 0.01 Pct Recovery = 105% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl SpecificMix = LB92783 Laboratory ID = 20130100066 Lab Value = 0.078 Expected Conc. = 0.075 Report level label = 0.01 Pct Recovery = 104% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl SpecificMix = LB92783 Laboratory ID = 20123560092 Lab Value = 0.064 Expected Conc. = 0.075 Report level label = 0.01 Pct Recovery = 86% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = 0507-12-04.2 Laboratory ID = 20172510330 Lab Value = 0.069 Expected Conc. = 0.067 Report level label = 0.01 Pct Recovery = 103% Analysis Date = 12/29/17 SpikeMix = ChemService 6537100: 100 µl & Abs 071817Pest: 100 µl SpecificMix = 071817Pest Laboratory ID = 20163370001 Lab Value = 0.064 Expected Conc. = 0.0625 Report level label = 0.01 Pct Recovery = 103% Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl SpecificMix = LC20138V Laboratory ID = 20162860079 Lab Value = 0.072 Expected Conc. = 0.06 Report level label = 0.01 Pct Recovery = 121% Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl SpecificMix = 5054800 Laboratory ID = 20161880109 Lab Value = 0.079 Expected Conc. = 0.06 Report level label = 0.01 Pct Recovery = 132% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl SpecificMix = 5054800 Laboratory ID = 20152750006 Lab Value = 0.053 Expected Conc. = 0.06 Report level label = 0.01 Pct Recovery = 88% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl SpecificMix = EN150514012 Laboratory ID = 20152460215 Lab Value = 0.063 Expected Conc. = 0.06 Report level label = 0.01 Pct Recovery = 105% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl SpecificMix = EN150514012 Laboratory ID = 20171720140 Lab Value = 0.051 Expected Conc. = 0.05 Report level label = 0.01 Pct Recovery = 102% Analysis Date = 08/31/17 SpikeMix = Supelco LC20138V: 80 µl & Phenova B20160331: 80 µl SpecificMix = LC20138V Laboratory ID = 20170740063 Lab Value = 0.048 Expected Conc. = 0.05 Report level label = 0.01 Pct Recovery = 97% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl SpecificMix = LC20138V Laboratory ID = 20161470001 Lab Value = 0.062 Expected Conc. = 0.05 Report level label = 0.01 Pct Recovery = 124% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl SpecificMix = LC20138V Laboratory ID = 20171380001 Lab Value = 0.043 Expected Conc. = 0.048 Report level label = 0.01 Pct Recovery = 90% Analysis Date = 06/07/17 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 5054800 Laboratory ID = 20170960001 Lab Value = 0.057 Expected Conc. = 0.048 Report level label = 0.01 Pct Recovery = 120% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl SpecificMix = 5054800 Laboratory ID = 20161740258 Lab Value = 0.037 Expected Conc. = 0.048 Report level label = 0.01 Pct Recovery = 77% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 5054800 Laboratory ID = 20143240095 Lab Value = 0.048 Expected Conc. = 0.0402 Report level label = 0.01 Pct Recovery = 120% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl SpecificMix = 032714 Laboratory ID = 20142270001 Lab Value = 0.036 Expected Conc. = 0.0402 Report level label = 0.01 Pct Recovery = 90% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl SpecificMix = 032714 Laboratory ID = 20141220025 Lab Value = 0.050 Expected Conc. = 0.0402 Report level label = 0.01 Pct Recovery = 124% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl SpecificMix = 032714 Laboratory ID = 20150430092 Lab Value = 0.040 Expected Conc. = 0.0401 Report level label = 0.01 Pct Recovery = 99% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl SpecificMix = E1140407002 Laboratory ID = 20143110108 Lab Value = 0.038 Expected Conc. = 0.0401 Report level label = 0.01 Pct Recovery = 95% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl SpecificMix = E1140407002 Laboratory ID = 20142720002 Lab Value = 0.036 Expected Conc. = 0.0401 Report level label = 0.01 Pct Recovery = 90% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl SpecificMix = E1140407002 Laboratory ID = 20141770149 Lab Value = 0.036 Expected Conc. = 0.0401 Report level label = 0.01 Pct Recovery = 89% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl SpecificMix = E1140407002 Laboratory ID = 20140510043 Lab Value = 0.028 Expected Conc. = 0.04 Report level label = 0.01 Pct Recovery = 70% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl SpecificMix = LB99392 Laboratory ID = 20133470008 Lab Value = 0.039 Expected Conc. = 0.04 Report level label = 0.01 Pct Recovery = 98% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl SpecificMix = LB99392 Laboratory ID = 20133190012 Lab Value = 0.045 Expected Conc. = 0.04 Report level label = 0.01 Pct Recovery = 113% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = LB99392 Laboratory ID = 20133050050 Lab Value = 0.041 Expected Conc. = 0.04 Report level label = 0.01 Pct Recovery = 103% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl SpecificMix = LB99392 Laboratory ID = 20133580036 Lab Value = 0.026 Expected Conc. = 0.0398 Report level label = 0.01 Pct Recovery = 64% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20131790009 Lab Value = 0.026 Expected Conc. = 0.0398 Report level label = 0.01 Pct Recovery = 66% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20131510026 Lab Value = 0.040 Expected Conc. = 0.0398 Report level label = 0.01 Pct Recovery = 101% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20173480003 Lab Value = 0.033 Expected Conc. = 0.035 Report level label = 0.01 Pct Recovery = 95% Analysis Date = 04/05/18 SpikeMix = Abs 071717Pest: 50 µl & ChemService 6567600: 50 µl SpecificMix = 6567600 Laboratory ID = 20172560101 Lab Value = 0.033 Expected Conc. = 0.035 Report level label = 0.01 Pct Recovery = 93% Analysis Date = 12/22/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6567600: 50 µl SpecificMix = 6567600 Laboratory ID = 20181430122 Lab Value = 0.042 Expected Conc. = 0.0335 Report level label = 0.01 Pct Recovery = 126% Analysis Date = 06/20/18 SpikeMix = Abs 071817Pest: 50 µl & Spex Organics EN170808006: 50 µl SpecificMix = 071817Pest Laboratory ID = 20160630046 Lab Value = 0.028 Expected Conc. = 0.03 Report level label = 0.01 Pct Recovery = 92% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = EN150514012 Laboratory ID = 20153440001 Lab Value = 0.022 Expected Conc. = 0.03 Report level label = 0.01 Pct Recovery = 72% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = EN150514012 Laboratory ID = 20152330039 Lab Value = 0.030 Expected Conc. = 0.03 Report level label = 0.01 Pct Recovery = 101% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl SpecificMix = 041415 Laboratory ID = 20151900132 Lab Value = 0.038 Expected Conc. = 0.03 Report level label = 0.01 Pct Recovery = 125% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl SpecificMix = 041415 Laboratory ID = 20151270112 Lab Value = 0.032 Expected Conc. = 0.03 Report level label = 0.01 Pct Recovery = 106% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl SpecificMix = 041415 Laboratory ID = 20130510051 Lab Value = 0.029 Expected Conc. = 0.03 Report level label = 0.01 Pct Recovery = 96% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl SpecificMix = 0507-12-04.2 Laboratory ID = 20130390105 Lab Value = 0.026 Expected Conc. = 0.03 Report level label = 0.01 Pct Recovery = 88% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl SpecificMix = LB92783 Laboratory ID = 20171510080 Lab Value = 0.029 Expected Conc. = 0.025 Report level label = 0.01 Pct Recovery = 115% Analysis Date = 06/09/17 SpikeMix = Supelco LC20138V: 40 µl & Crescent 03FF076: 40 µl SpecificMix = LC20138V Laboratory ID = 20162520001 Lab Value = 0.036 Expected Conc. = 0.025 Report level label = 0.01 Pct Recovery = 142% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl SpecificMix = LC20138V Laboratory ID = 20162660005 Lab Value = 0.025 Expected Conc. = 0.025 Report level label = 0.01 Pct Recovery = 98% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl SpecificMix = LC20138V Laboratory ID = 20162020124 Lab Value = 0.025 Expected Conc. = 0.025 Report level label = 0.01 Pct Recovery = 102% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl SpecificMix = LC20138V Laboratory ID = 20171940002 Lab Value = 0.034 Expected Conc. = 0.024 Report level label = 0.01 Pct Recovery = 141% Analysis Date = 11/10/17 SpikeMix = ChemService 5054800: 40 µl & NSI 041816: 40 µl SpecificMix = 5054800 Laboratory ID = 20170460061 Lab Value = 0.028 Expected Conc. = 0.024 Report level label = 0.01 Pct Recovery = 116% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl SpecificMix = 5054800 Laboratory ID = 20163560019 Lab Value = 0.022 Expected Conc. = 0.024 Report level label = 0.01 Pct Recovery = 91% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl SpecificMix = 5054800 Laboratory ID = 20162150213 Lab Value = 0.030 Expected Conc. = 0.024 Report level label = 0.01 Pct Recovery = 126% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl SpecificMix = 5054800 Laboratory ID = 20180730064 Lab Value = 0.025 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 125% Analysis Date = 05/16/18 SpikeMix = Abs 071717Pest: 30 µl & Abs 071817Pest: 30 µl SpecificMix = 071817Pest Laboratory ID = 20180050004 Lab Value = 0.024 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 118% Analysis Date = 04/05/18 SpikeMix = Abs 071817Pest: 30 µl & ChemService 6472100: 30 µl SpecificMix = 071817Pest Laboratory ID = 20172780018 Lab Value = 0.022 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 108% Analysis Date = 02/08/18 SpikeMix = ChemService 6537100: 30 µl & Abs 071817Pest: 30 µl SpecificMix = 071817Pest Laboratory ID = 20150150115 Lab Value = 0.020 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 98% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl SpecificMix = 032714 Laboratory ID = 20142820151 Lab Value = 0.022 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 111% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl SpecificMix = 032714 Laboratory ID = 20141490205 Lab Value = 0.027 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 133% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = 032714 Laboratory ID = 20141080004 Lab Value = 0.024 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 121% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl SpecificMix = 032714 Laboratory ID = 20142470041 Lab Value = 0.024 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 120% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141910243 Lab Value = 0.019 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 95% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141640076 Lab Value = 0.022 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 110% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141360094 Lab Value = 0.022 Expected Conc. = 0.0201 Report level label = 0.01 Pct Recovery = 108% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = E1140407002 Laboratory ID = 20161050143 Lab Value = 0.017 Expected Conc. = 0.015 Report level label = 0.01 Pct Recovery = 112% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 041415 Laboratory ID = 20160560044 Lab Value = 0.015 Expected Conc. = 0.015 Report level label = 0.01 Pct Recovery = 103% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl SpecificMix = 041415 Laboratory ID = 20160210080 Lab Value = 0.013 Expected Conc. = 0.015 Report level label = 0.01 Pct Recovery = 88% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 041415 Laboratory ID = 20160070059 Lab Value = 0.012 Expected Conc. = 0.015 Report level label = 0.01 Pct Recovery = 79% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = EN150514012 Laboratory ID = 20153160001 Lab Value = 0.015 Expected Conc. = 0.015 Report level label = 0.01 Pct Recovery = 102% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = EN150514012 Laboratory ID = 20152950078 Lab Value = 0.011 Expected Conc. = 0.015 Report level label = 0.01 Pct Recovery = 73% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 041415 Laboratory ID = 20152040177 Lab Value = 0.020 Expected Conc. = 0.015 Report level label = 0.01 Pct Recovery = 134% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl SpecificMix = 041415 Laboratory ID = 20151760208 Lab Value = 0.021 Expected Conc. = 0.015 Report level label = 0.01 Pct Recovery = 139% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl SpecificMix = EN150514012 Laboratory ID = 20151480170 Lab Value = 0.017 Expected Conc. = 0.015 Report level label = 0.01 Pct Recovery = 116% Analysis Date = 06/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150514012 Laboratory ID = 20151210037 Lab Value = 0.019 Expected Conc. = 0.015 Report level label = 0.01 Pct Recovery = 125% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 041415 Analysis Date = 06/19/18 Pct Recovery = 116% Analysis Date = 06/10/18 Pct Recovery = 116% Analysis Date = 06/10/18 Pct Recovery = 116% Analysis Date = 05/31/18 Pct Recovery = 116% Analysis Date = 05/31/18 Pct Recovery = 116% Analysis Date = 05/21/18 Pct Recovery = 115% Analysis Date = 05/21/18 Pct Recovery = 115% Analysis Date = 05/11/18 Pct Recovery = 115% Analysis Date = 05/11/18 Pct Recovery = 115% Analysis Date = 05/01/18 Pct Recovery = 115% Analysis Date = 05/01/18 Pct Recovery = 115% Analysis Date = 04/21/18 Pct Recovery = 115% Analysis Date = 04/21/18 Pct Recovery = 115% Analysis Date = 04/11/18 Pct Recovery = 115% Analysis Date = 04/11/18 Pct Recovery = 115% Analysis Date = 04/01/18 Pct Recovery = 115% Analysis Date = 04/01/18 Pct Recovery = 115% Analysis Date = 03/22/18 Pct Recovery = 114% Analysis Date = 03/22/18 Pct Recovery = 114% Analysis Date = 03/12/18 Pct Recovery = 114% Analysis Date = 03/12/18 Pct Recovery = 114% Analysis Date = 03/02/18 Pct Recovery = 114% Analysis Date = 03/02/18 Pct Recovery = 114% Analysis Date = 02/21/18 Pct Recovery = 114% Analysis Date = 02/21/18 Pct Recovery = 114% Analysis Date = 02/11/18 Pct Recovery = 114% Analysis Date = 02/11/18 Pct Recovery = 114% Analysis Date = 02/01/18 Pct Recovery = 114% Analysis Date = 02/01/18 Pct Recovery = 114% Analysis Date = 01/22/18 Pct Recovery = 113% Analysis Date = 01/22/18 Pct Recovery = 113% Analysis Date = 01/12/18 Pct Recovery = 113% Analysis Date = 01/12/18 Pct Recovery = 113% Analysis Date = 01/02/18 Pct Recovery = 113% Analysis Date = 01/02/18 Pct Recovery = 113% Analysis Date = 12/23/17 Pct Recovery = 113% Analysis Date = 12/23/17 Pct Recovery = 113% Analysis Date = 12/13/17 Pct Recovery = 113% Analysis Date = 12/13/17 Pct Recovery = 113% Analysis Date = 12/03/17 Pct Recovery = 113% Analysis Date = 12/03/17 Pct Recovery = 113% Analysis Date = 11/23/17 Pct Recovery = 112% Analysis Date = 11/23/17 Pct Recovery = 112% Analysis Date = 11/13/17 Pct Recovery = 112% Analysis Date = 11/13/17 Pct Recovery = 112% Analysis Date = 11/04/17 Pct Recovery = 112% Analysis Date = 11/04/17 Pct Recovery = 112% Analysis Date = 10/25/17 Pct Recovery = 112% Analysis Date = 10/25/17 Pct Recovery = 112% Analysis Date = 10/15/17 Pct Recovery = 112% Analysis Date = 10/15/17 Pct Recovery = 112% Analysis Date = 10/05/17 Pct Recovery = 111% Analysis Date = 10/05/17 Pct Recovery = 111% Analysis Date = 09/25/17 Pct Recovery = 111% Analysis Date = 09/25/17 Pct Recovery = 111% Analysis Date = 09/15/17 Pct Recovery = 111% Analysis Date = 09/15/17 Pct Recovery = 111% Analysis Date = 09/05/17 Pct Recovery = 111% Analysis Date = 09/05/17 Pct Recovery = 111% Analysis Date = 08/26/17 Pct Recovery = 111% Analysis Date = 08/26/17 Pct Recovery = 111% Analysis Date = 08/16/17 Pct Recovery = 111% Analysis Date = 08/16/17 Pct Recovery = 111% Analysis Date = 08/06/17 Pct Recovery = 110% Analysis Date = 08/06/17 Pct Recovery = 110% Analysis Date = 07/27/17 Pct Recovery = 110% Analysis Date = 07/27/17 Pct Recovery = 110% Analysis Date = 07/18/17 Pct Recovery = 110% Analysis Date = 07/18/17 Pct Recovery = 110% Analysis Date = 07/08/17 Pct Recovery = 110% Analysis Date = 07/08/17 Pct Recovery = 110% Analysis Date = 06/28/17 Pct Recovery = 110% Analysis Date = 06/28/17 Pct Recovery = 110% Analysis Date = 06/18/17 Pct Recovery = 110% Analysis Date = 06/18/17 Pct Recovery = 110% Analysis Date = 06/08/17 Pct Recovery = 109% Analysis Date = 06/08/17 Pct Recovery = 109% Analysis Date = 05/29/17 Pct Recovery = 109% Analysis Date = 05/29/17 Pct Recovery = 109% Analysis Date = 05/19/17 Pct Recovery = 109% Analysis Date = 05/19/17 Pct Recovery = 109% Analysis Date = 05/09/17 Pct Recovery = 109% Analysis Date = 05/09/17 Pct Recovery = 109% Analysis Date = 04/29/17 Pct Recovery = 109% Analysis Date = 04/29/17 Pct Recovery = 109% Analysis Date = 04/19/17 Pct Recovery = 108% Analysis Date = 04/19/17 Pct Recovery = 108% Analysis Date = 04/09/17 Pct Recovery = 108% Analysis Date = 04/09/17 Pct Recovery = 108% Analysis Date = 03/31/17 Pct Recovery = 108% Analysis Date = 03/31/17 Pct Recovery = 108% Analysis Date = 03/21/17 Pct Recovery = 108% Analysis Date = 03/21/17 Pct Recovery = 108% Analysis Date = 03/11/17 Pct Recovery = 108% Analysis Date = 03/11/17 Pct Recovery = 108% Analysis Date = 03/01/17 Pct Recovery = 108% Analysis Date = 03/01/17 Pct Recovery = 108% Analysis Date = 02/19/17 Pct Recovery = 107% Analysis Date = 02/19/17 Pct Recovery = 107% Analysis Date = 02/09/17 Pct Recovery = 107% Analysis Date = 02/09/17 Pct Recovery = 107% Analysis Date = 01/30/17 Pct Recovery = 107% Analysis Date = 01/30/17 Pct Recovery = 107% Analysis Date = 01/20/17 Pct Recovery = 107% Analysis Date = 01/20/17 Pct Recovery = 107% Analysis Date = 01/10/17 Pct Recovery = 107% Analysis Date = 01/10/17 Pct Recovery = 107% Analysis Date = 12/31/16 Pct Recovery = 107% Analysis Date = 12/31/16 Pct Recovery = 107% Analysis Date = 12/21/16 Pct Recovery = 107% Analysis Date = 12/21/16 Pct Recovery = 107% Analysis Date = 12/12/16 Pct Recovery = 106% Analysis Date = 12/12/16 Pct Recovery = 106% Analysis Date = 12/02/16 Pct Recovery = 106% Analysis Date = 12/02/16 Pct Recovery = 106% Analysis Date = 11/22/16 Pct Recovery = 106% Analysis Date = 11/22/16 Pct Recovery = 106% Analysis Date = 11/12/16 Pct Recovery = 106% Analysis Date = 11/12/16 Pct Recovery = 106% Analysis Date = 11/02/16 Pct Recovery = 106% Analysis Date = 11/02/16 Pct Recovery = 106% Analysis Date = 10/23/16 Pct Recovery = 106% Analysis Date = 10/23/16 Pct Recovery = 106% Analysis Date = 10/13/16 Pct Recovery = 106% Analysis Date = 10/13/16 Pct Recovery = 106% Analysis Date = 10/03/16 Pct Recovery = 106% Analysis Date = 10/03/16 Pct Recovery = 106% Analysis Date = 09/23/16 Pct Recovery = 105% Analysis Date = 09/23/16 Pct Recovery = 105% Analysis Date = 09/13/16 Pct Recovery = 105% Analysis Date = 09/13/16 Pct Recovery = 105% Analysis Date = 09/03/16 Pct Recovery = 105% Analysis Date = 09/03/16 Pct Recovery = 105% Analysis Date = 08/25/16 Pct Recovery = 105% Analysis Date = 08/25/16 Pct Recovery = 105% Analysis Date = 08/15/16 Pct Recovery = 105% Analysis Date = 08/15/16 Pct Recovery = 105% Analysis Date = 08/05/16 Pct Recovery = 105% Analysis Date = 08/05/16 Pct Recovery = 105% Analysis Date = 07/26/16 Pct Recovery = 105% Analysis Date = 07/26/16 Pct Recovery = 105% Analysis Date = 07/16/16 Pct Recovery = 105% Analysis Date = 07/16/16 Pct Recovery = 105% Analysis Date = 07/06/16 Pct Recovery = 105% Analysis Date = 07/06/16 Pct Recovery = 105% Analysis Date = 06/26/16 Pct Recovery = 105% Analysis Date = 06/26/16 Pct Recovery = 105% Analysis Date = 06/16/16 Pct Recovery = 105% Analysis Date = 06/16/16 Pct Recovery = 105% Analysis Date = 06/06/16 Pct Recovery = 105% Analysis Date = 06/06/16 Pct Recovery = 105% Analysis Date = 05/27/16 Pct Recovery = 105% Analysis Date = 05/27/16 Pct Recovery = 105% Analysis Date = 05/17/16 Pct Recovery = 105% Analysis Date = 05/17/16 Pct Recovery = 105% Analysis Date = 05/08/16 Pct Recovery = 105% Analysis Date = 05/08/16 Pct Recovery = 105% Analysis Date = 04/28/16 Pct Recovery = 105% Analysis Date = 04/28/16 Pct Recovery = 105% Analysis Date = 04/18/16 Pct Recovery = 105% Analysis Date = 04/18/16 Pct Recovery = 105% Analysis Date = 04/08/16 Pct Recovery = 105% Analysis Date = 04/08/16 Pct Recovery = 105% Analysis Date = 03/29/16 Pct Recovery = 105% Analysis Date = 03/29/16 Pct Recovery = 105% Analysis Date = 03/19/16 Pct Recovery = 105% Analysis Date = 03/19/16 Pct Recovery = 105% Analysis Date = 03/09/16 Pct Recovery = 105% Analysis Date = 03/09/16 Pct Recovery = 105% Analysis Date = 02/28/16 Pct Recovery = 105% Analysis Date = 02/28/16 Pct Recovery = 105% Analysis Date = 02/18/16 Pct Recovery = 105% Analysis Date = 02/18/16 Pct Recovery = 105% Analysis Date = 02/08/16 Pct Recovery = 105% Analysis Date = 02/08/16 Pct Recovery = 105% Analysis Date = 01/29/16 Pct Recovery = 105% Analysis Date = 01/29/16 Pct Recovery = 105% Analysis Date = 01/20/16 Pct Recovery = 105% Analysis Date = 01/20/16 Pct Recovery = 105% Analysis Date = 01/10/16 Pct Recovery = 105% Analysis Date = 01/10/16 Pct Recovery = 105% Analysis Date = 12/31/15 Pct Recovery = 105% Analysis Date = 12/31/15 Pct Recovery = 105% Analysis Date = 12/21/15 Pct Recovery = 105% Analysis Date = 12/21/15 Pct Recovery = 105% Analysis Date = 12/11/15 Pct Recovery = 105% Analysis Date = 12/11/15 Pct Recovery = 105% Analysis Date = 12/01/15 Pct Recovery = 105% Analysis Date = 12/01/15 Pct Recovery = 105% Analysis Date = 11/21/15 Pct Recovery = 105% Analysis Date = 11/21/15 Pct Recovery = 105% Analysis Date = 11/11/15 Pct Recovery = 105% Analysis Date = 11/11/15 Pct Recovery = 105% Analysis Date = 11/01/15 Pct Recovery = 105% Analysis Date = 11/01/15 Pct Recovery = 105% Analysis Date = 10/22/15 Pct Recovery = 105% Analysis Date = 10/22/15 Pct Recovery = 105% Analysis Date = 10/12/15 Pct Recovery = 105% Analysis Date = 10/12/15 Pct Recovery = 105% Analysis Date = 10/02/15 Pct Recovery = 105% Analysis Date = 10/02/15 Pct Recovery = 105% Analysis Date = 09/23/15 Pct Recovery = 105% Analysis Date = 09/23/15 Pct Recovery = 105% Analysis Date = 09/13/15 Pct Recovery = 105% Analysis Date = 09/13/15 Pct Recovery = 105% Analysis Date = 09/03/15 Pct Recovery = 105% Analysis Date = 09/03/15 Pct Recovery = 105% Analysis Date = 08/24/15 Pct Recovery = 105% Analysis Date = 08/24/15 Pct Recovery = 105% Analysis Date = 08/14/15 Pct Recovery = 105% Analysis Date = 08/14/15 Pct Recovery = 105% Analysis Date = 08/04/15 Pct Recovery = 105% Analysis Date = 08/04/15 Pct Recovery = 105% Analysis Date = 07/25/15 Pct Recovery = 105% Analysis Date = 07/25/15 Pct Recovery = 105% Analysis Date = 07/15/15 Pct Recovery = 105% Analysis Date = 07/15/15 Pct Recovery = 105% Analysis Date = 07/05/15 Pct Recovery = 105% Analysis Date = 07/05/15 Pct Recovery = 105% Analysis Date = 06/25/15 Pct Recovery = 105% Analysis Date = 06/25/15 Pct Recovery = 105% Analysis Date = 06/15/15 Pct Recovery = 105% Analysis Date = 06/15/15 Pct Recovery = 105% Analysis Date = 06/06/15 Pct Recovery = 105% Analysis Date = 06/06/15 Pct Recovery = 105% Analysis Date = 05/27/15 Pct Recovery = 105% Analysis Date = 05/27/15 Pct Recovery = 105% Analysis Date = 05/17/15 Pct Recovery = 105% Analysis Date = 05/17/15 Pct Recovery = 105% Analysis Date = 05/07/15 Pct Recovery = 105% Analysis Date = 05/07/15 Pct Recovery = 105% Analysis Date = 04/27/15 Pct Recovery = 105% Analysis Date = 04/27/15 Pct Recovery = 105% Analysis Date = 04/17/15 Pct Recovery = 105% Analysis Date = 04/17/15 Pct Recovery = 105% Analysis Date = 04/07/15 Pct Recovery = 105% Analysis Date = 04/07/15 Pct Recovery = 105% Analysis Date = 03/28/15 Pct Recovery = 106% Analysis Date = 03/28/15 Pct Recovery = 106% Analysis Date = 03/18/15 Pct Recovery = 106% Analysis Date = 03/18/15 Pct Recovery = 106% Analysis Date = 03/08/15 Pct Recovery = 106% Analysis Date = 03/08/15 Pct Recovery = 106% Analysis Date = 02/26/15 Pct Recovery = 106% Analysis Date = 02/26/15 Pct Recovery = 106% Analysis Date = 02/17/15 Pct Recovery = 106% Analysis Date = 02/17/15 Pct Recovery = 106% Analysis Date = 02/07/15 Pct Recovery = 106% Analysis Date = 02/07/15 Pct Recovery = 106% Analysis Date = 01/28/15 Pct Recovery = 106% Analysis Date = 01/28/15 Pct Recovery = 106% Analysis Date = 01/18/15 Pct Recovery = 106% Analysis Date = 01/18/15 Pct Recovery = 106% Analysis Date = 01/08/15 Pct Recovery = 106% Analysis Date = 01/08/15 Pct Recovery = 106% Analysis Date = 12/29/14 Pct Recovery = 106% Analysis Date = 12/29/14 Pct Recovery = 106% Analysis Date = 12/19/14 Pct Recovery = 106% Analysis Date = 12/19/14 Pct Recovery = 106% Analysis Date = 12/09/14 Pct Recovery = 106% Analysis Date = 12/09/14 Pct Recovery = 106% Analysis Date = 11/29/14 Pct Recovery = 106% Analysis Date = 11/29/14 Pct Recovery = 106% Analysis Date = 11/19/14 Pct Recovery = 106% Analysis Date = 11/19/14 Pct Recovery = 106% Analysis Date = 11/09/14 Pct Recovery = 105% Analysis Date = 11/09/14 Pct Recovery = 105% Analysis Date = 10/31/14 Pct Recovery = 105% Analysis Date = 10/31/14 Pct Recovery = 105% Analysis Date = 10/21/14 Pct Recovery = 105% Analysis Date = 10/21/14 Pct Recovery = 105% Analysis Date = 10/11/14 Pct Recovery = 105% Analysis Date = 10/11/14 Pct Recovery = 105% Analysis Date = 10/01/14 Pct Recovery = 105% Analysis Date = 10/01/14 Pct Recovery = 105% Analysis Date = 09/21/14 Pct Recovery = 105% Analysis Date = 09/21/14 Pct Recovery = 105% Analysis Date = 09/11/14 Pct Recovery = 104% Analysis Date = 09/11/14 Pct Recovery = 104% Analysis Date = 09/01/14 Pct Recovery = 104% Analysis Date = 09/01/14 Pct Recovery = 104% Analysis Date = 08/22/14 Pct Recovery = 104% Analysis Date = 08/22/14 Pct Recovery = 104% Analysis Date = 08/12/14 Pct Recovery = 103% Analysis Date = 08/12/14 Pct Recovery = 103% Analysis Date = 08/02/14 Pct Recovery = 103% Analysis Date = 08/02/14 Pct Recovery = 103% Analysis Date = 07/23/14 Pct Recovery = 103% Analysis Date = 07/23/14 Pct Recovery = 103% Analysis Date = 07/14/14 Pct Recovery = 102% Analysis Date = 07/14/14 Pct Recovery = 102% Analysis Date = 07/04/14 Pct Recovery = 102% Analysis Date = 07/04/14 Pct Recovery = 102% Analysis Date = 06/24/14 Pct Recovery = 102% Analysis Date = 06/24/14 Pct Recovery = 102% Analysis Date = 06/14/14 Pct Recovery = 101% Analysis Date = 06/14/14 Pct Recovery = 101% Analysis Date = 06/04/14 Pct Recovery = 101% Analysis Date = 06/04/14 Pct Recovery = 101% Analysis Date = 05/25/14 Pct Recovery = 101% Analysis Date = 05/25/14 Pct Recovery = 101% Analysis Date = 05/15/14 Pct Recovery = 100% Analysis Date = 05/15/14 Pct Recovery = 100% Analysis Date = 05/05/14 Pct Recovery = 100% Analysis Date = 05/05/14 Pct Recovery = 100% Analysis Date = 04/25/14 Pct Recovery = 100% Analysis Date = 04/25/14 Pct Recovery = 100% Analysis Date = 04/15/14 Pct Recovery = 100% Analysis Date = 04/15/14 Pct Recovery = 100% Analysis Date = 04/05/14 Pct Recovery = 99% Analysis Date = 04/05/14 Pct Recovery = 99% Analysis Date = 03/27/14 Pct Recovery = 99% Analysis Date = 03/27/14 Pct Recovery = 99% Analysis Date = 03/17/14 Pct Recovery = 99% Analysis Date = 03/17/14 Pct Recovery = 99% Analysis Date = 03/07/14 Pct Recovery = 99% Analysis Date = 03/07/14 Pct Recovery = 99% Analysis Date = 02/25/14 Pct Recovery = 98% Analysis Date = 02/25/14 Pct Recovery = 98% Analysis Date = 02/15/14 Pct Recovery = 98% Analysis Date = 02/15/14 Pct Recovery = 98% Analysis Date = 02/05/14 Pct Recovery = 98% Analysis Date = 02/05/14 Pct Recovery = 98% Analysis Date = 01/26/14 Pct Recovery = 98% Analysis Date = 01/26/14 Pct Recovery = 98% Analysis Date = 01/16/14 Pct Recovery = 97% Analysis Date = 01/16/14 Pct Recovery = 97% Analysis Date = 01/06/14 Pct Recovery = 97% Analysis Date = 01/06/14 Pct Recovery = 97% Analysis Date = 12/27/13 Pct Recovery = 97% Analysis Date = 12/27/13 Pct Recovery = 97% Analysis Date = 12/17/13 Pct Recovery = 97% Analysis Date = 12/17/13 Pct Recovery = 97% Analysis Date = 12/08/13 Pct Recovery = 96% Analysis Date = 12/08/13 Pct Recovery = 96% Analysis Date = 11/28/13 Pct Recovery = 96% Analysis Date = 11/28/13 Pct Recovery = 96% Analysis Date = 11/18/13 Pct Recovery = 96% Analysis Date = 11/18/13 Pct Recovery = 96% Analysis Date = 11/08/13 Pct Recovery = 96% Analysis Date = 11/08/13 Pct Recovery = 96% Analysis Date = 10/29/13 Pct Recovery = 95% Analysis Date = 10/29/13 Pct Recovery = 95% Analysis Date = 10/19/13 Pct Recovery = 95% Analysis Date = 10/19/13 Pct Recovery = 95% Analysis Date = 10/09/13 Pct Recovery = 95% Analysis Date = 10/09/13 Pct Recovery = 95% Analysis Date = 09/29/13 Pct Recovery = 95% Analysis Date = 09/29/13 Pct Recovery = 95% Analysis Date = 09/19/13 Pct Recovery = 95% Analysis Date = 09/19/13 Pct Recovery = 95% Analysis Date = 09/09/13 Pct Recovery = 94% Analysis Date = 09/09/13 Pct Recovery = 94% Analysis Date = 08/30/13 Pct Recovery = 94% Analysis Date = 08/30/13 Pct Recovery = 94% Analysis Date = 08/21/13 Pct Recovery = 94% Analysis Date = 08/21/13 Pct Recovery = 94% Analysis Date = 08/11/13 Pct Recovery = 94% Analysis Date = 08/11/13 Pct Recovery = 94% Analysis Date = 08/01/13 Pct Recovery = 93% Analysis Date = 08/01/13 Pct Recovery = 93% Analysis Date = 07/22/13 Pct Recovery = 93% Analysis Date = 07/22/13 Pct Recovery = 93% Analysis Date = 07/12/13 Pct Recovery = 93% Analysis Date = 07/12/13 Pct Recovery = 93% Analysis Date = 07/02/13 Pct Recovery = 93% Analysis Date = 07/02/13 Pct Recovery = 93% Analysis Date = 06/22/13 Pct Recovery = 92% Analysis Date = 06/22/13 Pct Recovery = 92% Analysis Date = 06/12/13 Pct Recovery = 92% Analysis Date = 06/12/13 Pct Recovery = 92% Analysis Date = 06/02/13 Pct Recovery = 92% Analysis Date = 06/02/13 Pct Recovery = 92% Analysis Date = 05/23/13 Pct Recovery = 92% Analysis Date = 05/23/13 Pct Recovery = 92% Analysis Date = 05/13/13 Pct Recovery = 91% Analysis Date = 05/13/13 Pct Recovery = 91% Analysis Date = 05/04/13 Pct Recovery = 91% Analysis Date = 05/04/13 Pct Recovery = 91% Analysis Date = 04/24/13 Pct Recovery = 91% Analysis Date = 04/24/13 Pct Recovery = 91% Analysis Date = 04/14/13 Pct Recovery = 91% Analysis Date = 04/14/13 Pct Recovery = 91% Analysis Date = 04/04/13 Pct Recovery = 90% Analysis Date = 04/04/13 Pct Recovery = 90% Analysis Date = 03/25/13 Pct Recovery = 90% Analysis Date = 03/25/13 Pct Recovery = 90% Analysis Date = 03/15/13 Pct Recovery = 90% Analysis Date = 03/15/13 Pct Recovery = 90% Analysis Date = 03/05/13 Pct Recovery = 90% Analysis Date = 03/05/13 Pct Recovery = 90% Analysis Date = 02/23/13 Pct Recovery = 90% Analysis Date = 02/23/13 Pct Recovery = 90% Analysis Date = 02/13/13 Pct Recovery = 89% Analysis Date = 02/13/13 Pct Recovery = 89% Analysis Date = 02/03/13 Pct Recovery = 89% Analysis Date = 02/03/13 Pct Recovery = 89% Analysis Date = 01/24/13 Pct Recovery = 89% Analysis Date = 01/24/13 Pct Recovery = 89% Analysis Date = 01/15/13 Pct Recovery = 89% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
PROPANIL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 74 103% 18% 102% 20%
Total 74 103% 18% 102% 20%

Sample Statistics
PROPANIL

Characteristic N % % Basis
Plotted 74 100% Spiked
Estimated Values 1 1% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 74 .  
False Negatives 0 0% 0 out of 74
Not Spiked 60 .  
False Positives 0 0% 0 out of 60

OBSP Determination:
PROPARGITE
METHOD: 2033 , TESTIDCODE: 82685GCM35

Laboratory ID = 20130250061 Lab Value = 0.503 Expected Conc. = 0.5 Report level label = 0.02 Pct Recovery = 101% Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl SpecificMix = 05BB029 Laboratory ID = 20140100085 Lab Value = 0.219 Expected Conc. = 0.251 Report level label = 0.02 Pct Recovery = 87% Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl SpecificMix = 042413 Laboratory ID = 20130940097 Lab Value = 0.147 Expected Conc. = 0.251 Report level label = 0.02 Pct Recovery = 59% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = 052412 Laboratory ID = 20130100066 Lab Value = 0.465 Expected Conc. = 0.251 Report level label = 0.02 Pct Recovery = 185% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl SpecificMix = 052412 Laboratory ID = 20140230082 Lab Value = 0.140 Expected Conc. = 0.2505 Report level label = 0.02 Pct Recovery = 56% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl SpecificMix = 012513 Laboratory ID = 20132420001 Lab Value = 0.131 Expected Conc. = 0.2505 Report level label = 0.02 Pct Recovery = 52% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl SpecificMix = 012513 Laboratory ID = 20172510330 Lab Value = 0.097 Expected Conc. = 0.132 Report level label = 0.02 Pct Recovery = 73% Analysis Date = 12/29/17 SpikeMix = ChemService 6537100: 100 µl & Abs 071817Pest: 100 µl SpecificMix = 6537100 Laboratory ID = 20132690010 Lab Value = 0.118 Expected Conc. = 0.1255 Report level label = 0.02 Pct Recovery = 94% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl SpecificMix = 042413 Laboratory ID = 20132560001 Lab Value = 0.091 Expected Conc. = 0.1255 Report level label = 0.02 Pct Recovery = 72% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl SpecificMix = 042413 Laboratory ID = 20132140002 Lab Value = 0.082 Expected Conc. = 0.125 Report level label = 0.02 Pct Recovery = 66% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl SpecificMix = 04CC101 Laboratory ID = 20162860079 Lab Value = 0.104 Expected Conc. = 0.12 Report level label = 0.02 Pct Recovery = 87% Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl SpecificMix = 5054800 Laboratory ID = 20161880109 Lab Value = 0.131 Expected Conc. = 0.12 Report level label = 0.02 Pct Recovery = 109% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl SpecificMix = 5054800 Laboratory ID = 20152750006 Lab Value = 0.130 Expected Conc. = 0.12 Report level label = 0.02 Pct Recovery = 108% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl SpecificMix = 040615 Laboratory ID = 20152610011 Lab Value = 0.107 Expected Conc. = 0.12 Report level label = 0.02 Pct Recovery = 89% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl SpecificMix = 040615 Laboratory ID = 20133400002 Lab Value = 0.067 Expected Conc. = 0.1004 Report level label = 0.02 Pct Recovery = 67% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = 052412 Laboratory ID = 20132910008 Lab Value = 0.060 Expected Conc. = 0.1004 Report level label = 0.02 Pct Recovery = 59% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = 052412 Laboratory ID = 20130650005 Lab Value = 0.056 Expected Conc. = 0.1004 Report level label = 0.02 Pct Recovery = 56% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl SpecificMix = 052412 Laboratory ID = 20140860102 Lab Value = 0.061 Expected Conc. = 0.1002 Report level label = 0.02 Pct Recovery = 61% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 012513 Laboratory ID = 20131920149 Lab Value = 0.066 Expected Conc. = 0.1002 Report level label = 0.02 Pct Recovery = 66% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl SpecificMix = 012513 Laboratory ID = 20131230084 Lab Value = 0.088 Expected Conc. = 0.1 Report level label = 0.02 Pct Recovery = 87% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl SpecificMix = 05BB029 Laboratory ID = 20130510051 Lab Value = 0.055 Expected Conc. = 0.1 Report level label = 0.02 Pct Recovery = 55% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl SpecificMix = 05BB029 Laboratory ID = 20171380001 Lab Value = 0.068 Expected Conc. = 0.096 Report level label = 0.02 Pct Recovery = 71% Analysis Date = 06/07/17 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 5054800 Laboratory ID = 20170960001 Lab Value = 0.067 Expected Conc. = 0.096 Report level label = 0.02 Pct Recovery = 69% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl SpecificMix = 5054800 Laboratory ID = 20161740258 Lab Value = 0.055 Expected Conc. = 0.096 Report level label = 0.02 Pct Recovery = 57% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 5054800 Laboratory ID = 20150720069 Lab Value = 0.071 Expected Conc. = 0.0804 Report level label = 0.02 Pct Recovery = 88% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 0227-14-08 Laboratory ID = 20141770149 Lab Value = 0.055 Expected Conc. = 0.0804 Report level label = 0.02 Pct Recovery = 69% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl SpecificMix = 0227-14-08 Laboratory ID = 20141570088 Lab Value = 0.065 Expected Conc. = 0.0804 Report level label = 0.02 Pct Recovery = 81% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl SpecificMix = 0227-14-08 Laboratory ID = 20172230001 Lab Value = 0.062 Expected Conc. = 0.067 Report level label = 0.02 Pct Recovery = 93% Analysis Date = 10/19/17 SpikeMix = ChemService 6472100: 50 µl & Abs 071717Pest: 50 µl SpecificMix = 071717Pest Laboratory ID = 20172370001 Lab Value = 0.064 Expected Conc. = 0.066 Report level label = 0.02 Pct Recovery = 97% Analysis Date = 11/18/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6537100: 50 µl SpecificMix = 6537100 Laboratory ID = 20161260151 Lab Value = 0.045 Expected Conc. = 0.06 Report level label = 0.02 Pct Recovery = 75% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = EN150513008 Laboratory ID = 20160770090 Lab Value = 0.043 Expected Conc. = 0.06 Report level label = 0.02 Pct Recovery = 72% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = EN150513008 Laboratory ID = 20153510109 Lab Value = 0.043 Expected Conc. = 0.06 Report level label = 0.02 Pct Recovery = 72% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = EN150513008 Laboratory ID = 20152330039 Lab Value = 0.043 Expected Conc. = 0.06 Report level label = 0.02 Pct Recovery = 72% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl SpecificMix = EN150513008 Laboratory ID = 20151900132 Lab Value = 0.079 Expected Conc. = 0.06 Report level label = 0.02 Pct Recovery = 131% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl SpecificMix = 040615 Laboratory ID = 20151550293 Lab Value = 0.054 Expected Conc. = 0.06 Report level label = 0.02 Pct Recovery = 90% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl SpecificMix = 040615 Laboratory ID = 20172020035 Lab Value = 0.056 Expected Conc. = 0.0536 Report level label = 0.02 Pct Recovery = 104% Analysis Date = 11/07/17 SpikeMix = Abs 071717Pest: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 071717Pest Laboratory ID = 20133580036 Lab Value = 0.031 Expected Conc. = 0.0502 Report level label = 0.02 Pct Recovery = 62% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 042413 Laboratory ID = 20133190012 Lab Value = 0.041 Expected Conc. = 0.0502 Report level label = 0.02 Pct Recovery = 82% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 042413 Laboratory ID = 20131650073 Lab Value = 0.052 Expected Conc. = 0.0502 Report level label = 0.02 Pct Recovery = 104% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl SpecificMix = 042413 Laboratory ID = 20140730138 Lab Value = 0.033 Expected Conc. = 0.05 Report level label = 0.02 Pct Recovery = 65% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 04CC101 Laboratory ID = 20140510043 Lab Value = 0.044 Expected Conc. = 0.05 Report level label = 0.02 Pct Recovery = 89% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 04CC101 Laboratory ID = 20133310030 Lab Value = 0.043 Expected Conc. = 0.05 Report level label = 0.02 Pct Recovery = 85% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl SpecificMix = 04CC101 Laboratory ID = 20132280016 Lab Value = 0.050 Expected Conc. = 0.05 Report level label = 0.02 Pct Recovery = 100% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl SpecificMix = 04CC101 Laboratory ID = 20131510026 Lab Value = 0.045 Expected Conc. = 0.05 Report level label = 0.02 Pct Recovery = 89% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl SpecificMix = 04CC101 Laboratory ID = 20171940002 Lab Value = 0.047 Expected Conc. = 0.048 Report level label = 0.02 Pct Recovery = 98% Analysis Date = 11/10/17 SpikeMix = ChemService 5054800: 40 µl & NSI 041816: 40 µl SpecificMix = 5054800 Laboratory ID = 20170460061 Lab Value = 0.035 Expected Conc. = 0.048 Report level label = 0.02 Pct Recovery = 74% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl SpecificMix = 5054800 Laboratory ID = 20163560019 Lab Value = 0.047 Expected Conc. = 0.048 Report level label = 0.02 Pct Recovery = 97% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl SpecificMix = 5054800 Laboratory ID = 20162150213 Lab Value = 0.052 Expected Conc. = 0.048 Report level label = 0.02 Pct Recovery = 108% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl SpecificMix = 5054800 Laboratory ID = 20141840097 Lab Value = 0.033 Expected Conc. = 0.0402 Report level label = 0.02 Pct Recovery = 83% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20141490205 Lab Value = 0.031 Expected Conc. = 0.0402 Report level label = 0.02 Pct Recovery = 77% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20141420140 Lab Value = 0.038 Expected Conc. = 0.0402 Report level label = 0.02 Pct Recovery = 95% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20141360094 Lab Value = 0.022 Expected Conc. = 0.0402 Report level label = 0.02 Pct Recovery = 55% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20173120093 Lab Value = 0.037 Expected Conc. = 0.0396 Report level label = 0.02 Pct Recovery = 93% Analysis Date = 03/10/18 SpikeMix = ChemService 6472100: 30 µl & ChemService 6537100: 30 µl SpecificMix = 6537100 Laboratory ID = 20161050143 Lab Value = 0.023 Expected Conc. = 0.03 Report level label = 0.02 Pct Recovery = 75% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Laboratory ID = 20160430111 Lab Value = 0.027 Expected Conc. = 0.03 Report level label = 0.02 Pct Recovery = 90% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Laboratory ID = 20160560044 Lab Value = 0.022 Expected Conc. = 0.03 Report level label = 0.02 Pct Recovery = 72% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl SpecificMix = EN150513008 Laboratory ID = 20160070059 Lab Value = 0.025 Expected Conc. = 0.03 Report level label = 0.02 Pct Recovery = 82% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = 040615 Laboratory ID = 20153160001 Lab Value = 0.023 Expected Conc. = 0.03 Report level label = 0.02 Pct Recovery = 76% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = EN150513008 Laboratory ID = 20153030068 Lab Value = 0.023 Expected Conc. = 0.03 Report level label = 0.02 Pct Recovery = 77% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150513008 Laboratory ID = 20152190003 Lab Value = 0.025 Expected Conc. = 0.03 Report level label = 0.02 Pct Recovery = 82% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150513008 Laboratory ID = 20151480170 Lab Value = 0.024 Expected Conc. = 0.03 Report level label = 0.02 Pct Recovery = 80% Analysis Date = 06/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150513008 Laboratory ID = 20151380009 Lab Value = 0.023 Expected Conc. = 0.03 Report level label = 0.02 Pct Recovery = 78% Analysis Date = 05/30/15 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Laboratory ID = 20151210037 Lab Value = 0.026 Expected Conc. = 0.03 Report level label = 0.02 Pct Recovery = 87% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Analysis Date = 03/09/18 Pct Recovery = 89% Analysis Date = 02/28/18 Pct Recovery = 89% Analysis Date = 02/28/18 Pct Recovery = 89% Analysis Date = 02/19/18 Pct Recovery = 89% Analysis Date = 02/19/18 Pct Recovery = 89% Analysis Date = 02/09/18 Pct Recovery = 89% Analysis Date = 02/09/18 Pct Recovery = 89% Analysis Date = 01/31/18 Pct Recovery = 89% Analysis Date = 01/31/18 Pct Recovery = 89% Analysis Date = 01/22/18 Pct Recovery = 89% Analysis Date = 01/22/18 Pct Recovery = 89% Analysis Date = 01/12/18 Pct Recovery = 89% Analysis Date = 01/12/18 Pct Recovery = 89% Analysis Date = 01/03/18 Pct Recovery = 88% Analysis Date = 01/03/18 Pct Recovery = 88% Analysis Date = 12/24/17 Pct Recovery = 88% Analysis Date = 12/24/17 Pct Recovery = 88% Analysis Date = 12/15/17 Pct Recovery = 88% Analysis Date = 12/15/17 Pct Recovery = 88% Analysis Date = 12/06/17 Pct Recovery = 88% Analysis Date = 12/06/17 Pct Recovery = 88% Analysis Date = 11/26/17 Pct Recovery = 88% Analysis Date = 11/26/17 Pct Recovery = 88% Analysis Date = 11/17/17 Pct Recovery = 88% Analysis Date = 11/17/17 Pct Recovery = 88% Analysis Date = 11/07/17 Pct Recovery = 88% Analysis Date = 11/07/17 Pct Recovery = 88% Analysis Date = 10/29/17 Pct Recovery = 88% Analysis Date = 10/29/17 Pct Recovery = 88% Analysis Date = 10/20/17 Pct Recovery = 88% Analysis Date = 10/20/17 Pct Recovery = 88% Analysis Date = 10/10/17 Pct Recovery = 88% Analysis Date = 10/10/17 Pct Recovery = 88% Analysis Date = 10/01/17 Pct Recovery = 88% Analysis Date = 10/01/17 Pct Recovery = 88% Analysis Date = 09/21/17 Pct Recovery = 88% Analysis Date = 09/21/17 Pct Recovery = 88% Analysis Date = 09/12/17 Pct Recovery = 88% Analysis Date = 09/12/17 Pct Recovery = 88% Analysis Date = 09/03/17 Pct Recovery = 88% Analysis Date = 09/03/17 Pct Recovery = 88% Analysis Date = 08/24/17 Pct Recovery = 87% Analysis Date = 08/24/17 Pct Recovery = 87% Analysis Date = 08/15/17 Pct Recovery = 87% Analysis Date = 08/15/17 Pct Recovery = 87% Analysis Date = 08/06/17 Pct Recovery = 87% Analysis Date = 08/06/17 Pct Recovery = 87% Analysis Date = 07/27/17 Pct Recovery = 87% Analysis Date = 07/27/17 Pct Recovery = 87% Analysis Date = 07/18/17 Pct Recovery = 87% Analysis Date = 07/18/17 Pct Recovery = 87% Analysis Date = 07/08/17 Pct Recovery = 87% Analysis Date = 07/08/17 Pct Recovery = 87% Analysis Date = 06/29/17 Pct Recovery = 87% Analysis Date = 06/29/17 Pct Recovery = 87% Analysis Date = 06/20/17 Pct Recovery = 87% Analysis Date = 06/20/17 Pct Recovery = 87% Analysis Date = 06/10/17 Pct Recovery = 87% Analysis Date = 06/10/17 Pct Recovery = 87% Analysis Date = 06/01/17 Pct Recovery = 87% Analysis Date = 06/01/17 Pct Recovery = 87% Analysis Date = 05/22/17 Pct Recovery = 87% Analysis Date = 05/22/17 Pct Recovery = 87% Analysis Date = 05/13/17 Pct Recovery = 87% Analysis Date = 05/13/17 Pct Recovery = 87% Analysis Date = 05/04/17 Pct Recovery = 87% Analysis Date = 05/04/17 Pct Recovery = 87% Analysis Date = 04/24/17 Pct Recovery = 86% Analysis Date = 04/24/17 Pct Recovery = 86% Analysis Date = 04/15/17 Pct Recovery = 86% Analysis Date = 04/15/17 Pct Recovery = 86% Analysis Date = 04/05/17 Pct Recovery = 86% Analysis Date = 04/05/17 Pct Recovery = 86% Analysis Date = 03/27/17 Pct Recovery = 86% Analysis Date = 03/27/17 Pct Recovery = 86% Analysis Date = 03/18/17 Pct Recovery = 86% Analysis Date = 03/18/17 Pct Recovery = 86% Analysis Date = 03/08/17 Pct Recovery = 86% Analysis Date = 03/08/17 Pct Recovery = 86% Analysis Date = 02/27/17 Pct Recovery = 86% Analysis Date = 02/27/17 Pct Recovery = 86% Analysis Date = 02/18/17 Pct Recovery = 86% Analysis Date = 02/18/17 Pct Recovery = 86% Analysis Date = 02/08/17 Pct Recovery = 86% Analysis Date = 02/08/17 Pct Recovery = 86% Analysis Date = 01/30/17 Pct Recovery = 86% Analysis Date = 01/30/17 Pct Recovery = 86% Analysis Date = 01/20/17 Pct Recovery = 86% Analysis Date = 01/20/17 Pct Recovery = 86% Analysis Date = 01/11/17 Pct Recovery = 86% Analysis Date = 01/11/17 Pct Recovery = 86% Analysis Date = 01/02/17 Pct Recovery = 86% Analysis Date = 01/02/17 Pct Recovery = 86% Analysis Date = 12/23/16 Pct Recovery = 86% Analysis Date = 12/23/16 Pct Recovery = 86% Analysis Date = 12/14/16 Pct Recovery = 86% Analysis Date = 12/14/16 Pct Recovery = 86% Analysis Date = 12/04/16 Pct Recovery = 86% Analysis Date = 12/04/16 Pct Recovery = 86% Analysis Date = 11/25/16 Pct Recovery = 85% Analysis Date = 11/25/16 Pct Recovery = 85% Analysis Date = 11/16/16 Pct Recovery = 85% Analysis Date = 11/16/16 Pct Recovery = 85% Analysis Date = 11/06/16 Pct Recovery = 85% Analysis Date = 11/06/16 Pct Recovery = 85% Analysis Date = 10/28/16 Pct Recovery = 85% Analysis Date = 10/28/16 Pct Recovery = 85% Analysis Date = 10/18/16 Pct Recovery = 85% Analysis Date = 10/18/16 Pct Recovery = 85% Analysis Date = 10/09/16 Pct Recovery = 85% Analysis Date = 10/09/16 Pct Recovery = 85% Analysis Date = 09/30/16 Pct Recovery = 85% Analysis Date = 09/30/16 Pct Recovery = 85% Analysis Date = 09/20/16 Pct Recovery = 85% Analysis Date = 09/20/16 Pct Recovery = 85% Analysis Date = 09/11/16 Pct Recovery = 85% Analysis Date = 09/11/16 Pct Recovery = 85% Analysis Date = 09/01/16 Pct Recovery = 85% Analysis Date = 09/01/16 Pct Recovery = 85% Analysis Date = 08/23/16 Pct Recovery = 85% Analysis Date = 08/23/16 Pct Recovery = 85% Analysis Date = 08/14/16 Pct Recovery = 85% Analysis Date = 08/14/16 Pct Recovery = 85% Analysis Date = 08/04/16 Pct Recovery = 85% Analysis Date = 08/04/16 Pct Recovery = 85% Analysis Date = 07/26/16 Pct Recovery = 85% Analysis Date = 07/26/16 Pct Recovery = 85% Analysis Date = 07/17/16 Pct Recovery = 85% Analysis Date = 07/17/16 Pct Recovery = 85% Analysis Date = 07/07/16 Pct Recovery = 85% Analysis Date = 07/07/16 Pct Recovery = 85% Analysis Date = 06/28/16 Pct Recovery = 84% Analysis Date = 06/28/16 Pct Recovery = 84% Analysis Date = 06/18/16 Pct Recovery = 84% Analysis Date = 06/18/16 Pct Recovery = 84% Analysis Date = 06/09/16 Pct Recovery = 84% Analysis Date = 06/09/16 Pct Recovery = 84% Analysis Date = 05/31/16 Pct Recovery = 84% Analysis Date = 05/31/16 Pct Recovery = 84% Analysis Date = 05/21/16 Pct Recovery = 84% Analysis Date = 05/21/16 Pct Recovery = 84% Analysis Date = 05/12/16 Pct Recovery = 84% Analysis Date = 05/12/16 Pct Recovery = 84% Analysis Date = 05/02/16 Pct Recovery = 84% Analysis Date = 05/02/16 Pct Recovery = 84% Analysis Date = 04/23/16 Pct Recovery = 84% Analysis Date = 04/23/16 Pct Recovery = 84% Analysis Date = 04/14/16 Pct Recovery = 84% Analysis Date = 04/14/16 Pct Recovery = 84% Analysis Date = 04/04/16 Pct Recovery = 84% Analysis Date = 04/04/16 Pct Recovery = 84% Analysis Date = 03/26/16 Pct Recovery = 84% Analysis Date = 03/26/16 Pct Recovery = 84% Analysis Date = 03/16/16 Pct Recovery = 84% Analysis Date = 03/16/16 Pct Recovery = 84% Analysis Date = 03/07/16 Pct Recovery = 84% Analysis Date = 03/07/16 Pct Recovery = 84% Analysis Date = 02/27/16 Pct Recovery = 84% Analysis Date = 02/27/16 Pct Recovery = 84% Analysis Date = 02/17/16 Pct Recovery = 85% Analysis Date = 02/17/16 Pct Recovery = 85% Analysis Date = 02/08/16 Pct Recovery = 85% Analysis Date = 02/08/16 Pct Recovery = 85% Analysis Date = 01/30/16 Pct Recovery = 85% Analysis Date = 01/30/16 Pct Recovery = 85% Analysis Date = 01/20/16 Pct Recovery = 85% Analysis Date = 01/20/16 Pct Recovery = 85% Analysis Date = 01/11/16 Pct Recovery = 85% Analysis Date = 01/11/16 Pct Recovery = 85% Analysis Date = 01/01/16 Pct Recovery = 85% Analysis Date = 01/01/16 Pct Recovery = 85% Analysis Date = 12/23/15 Pct Recovery = 84% Analysis Date = 12/23/15 Pct Recovery = 84% Analysis Date = 12/14/15 Pct Recovery = 84% Analysis Date = 12/14/15 Pct Recovery = 84% Analysis Date = 12/04/15 Pct Recovery = 84% Analysis Date = 12/04/15 Pct Recovery = 84% Analysis Date = 11/25/15 Pct Recovery = 84% Analysis Date = 11/25/15 Pct Recovery = 84% Analysis Date = 11/15/15 Pct Recovery = 84% Analysis Date = 11/15/15 Pct Recovery = 84% Analysis Date = 11/06/15 Pct Recovery = 84% Analysis Date = 11/06/15 Pct Recovery = 84% Analysis Date = 10/28/15 Pct Recovery = 84% Analysis Date = 10/28/15 Pct Recovery = 84% Analysis Date = 10/18/15 Pct Recovery = 84% Analysis Date = 10/18/15 Pct Recovery = 84% Analysis Date = 10/09/15 Pct Recovery = 84% Analysis Date = 10/09/15 Pct Recovery = 84% Analysis Date = 09/29/15 Pct Recovery = 84% Analysis Date = 09/29/15 Pct Recovery = 84% Analysis Date = 09/20/15 Pct Recovery = 84% Analysis Date = 09/20/15 Pct Recovery = 84% Analysis Date = 09/11/15 Pct Recovery = 84% Analysis Date = 09/11/15 Pct Recovery = 84% Analysis Date = 09/01/15 Pct Recovery = 84% Analysis Date = 09/01/15 Pct Recovery = 84% Analysis Date = 08/23/15 Pct Recovery = 84% Analysis Date = 08/23/15 Pct Recovery = 84% Analysis Date = 08/13/15 Pct Recovery = 84% Analysis Date = 08/13/15 Pct Recovery = 84% Analysis Date = 08/04/15 Pct Recovery = 84% Analysis Date = 08/04/15 Pct Recovery = 84% Analysis Date = 07/26/15 Pct Recovery = 84% Analysis Date = 07/26/15 Pct Recovery = 84% Analysis Date = 07/16/15 Pct Recovery = 84% Analysis Date = 07/16/15 Pct Recovery = 84% Analysis Date = 07/07/15 Pct Recovery = 84% Analysis Date = 07/07/15 Pct Recovery = 84% Analysis Date = 06/28/15 Pct Recovery = 84% Analysis Date = 06/28/15 Pct Recovery = 84% Analysis Date = 06/18/15 Pct Recovery = 84% Analysis Date = 06/18/15 Pct Recovery = 84% Analysis Date = 06/09/15 Pct Recovery = 84% Analysis Date = 06/09/15 Pct Recovery = 84% Analysis Date = 05/30/15 Pct Recovery = 84% Analysis Date = 05/30/15 Pct Recovery = 84% Analysis Date = 05/21/15 Pct Recovery = 83% Analysis Date = 05/21/15 Pct Recovery = 83% Analysis Date = 05/12/15 Pct Recovery = 83% Analysis Date = 05/12/15 Pct Recovery = 83% Analysis Date = 05/02/15 Pct Recovery = 83% Analysis Date = 05/02/15 Pct Recovery = 83% Analysis Date = 04/23/15 Pct Recovery = 83% Analysis Date = 04/23/15 Pct Recovery = 83% Analysis Date = 04/13/15 Pct Recovery = 83% Analysis Date = 04/13/15 Pct Recovery = 83% Analysis Date = 04/04/15 Pct Recovery = 83% Analysis Date = 04/04/15 Pct Recovery = 83% Analysis Date = 03/26/15 Pct Recovery = 82% Analysis Date = 03/26/15 Pct Recovery = 82% Analysis Date = 03/16/15 Pct Recovery = 82% Analysis Date = 03/16/15 Pct Recovery = 82% Analysis Date = 03/07/15 Pct Recovery = 82% Analysis Date = 03/07/15 Pct Recovery = 82% Analysis Date = 02/25/15 Pct Recovery = 82% Analysis Date = 02/25/15 Pct Recovery = 82% Analysis Date = 02/16/15 Pct Recovery = 82% Analysis Date = 02/16/15 Pct Recovery = 82% Analysis Date = 02/07/15 Pct Recovery = 82% Analysis Date = 02/07/15 Pct Recovery = 82% Analysis Date = 01/28/15 Pct Recovery = 81% Analysis Date = 01/28/15 Pct Recovery = 81% Analysis Date = 01/19/15 Pct Recovery = 81% Analysis Date = 01/19/15 Pct Recovery = 81% Analysis Date = 01/10/15 Pct Recovery = 81% Analysis Date = 01/10/15 Pct Recovery = 81% Analysis Date = 12/31/14 Pct Recovery = 81% Analysis Date = 12/31/14 Pct Recovery = 81% Analysis Date = 12/22/14 Pct Recovery = 81% Analysis Date = 12/22/14 Pct Recovery = 81% Analysis Date = 12/12/14 Pct Recovery = 80% Analysis Date = 12/12/14 Pct Recovery = 80% Analysis Date = 12/03/14 Pct Recovery = 80% Analysis Date = 12/03/14 Pct Recovery = 80% Analysis Date = 11/24/14 Pct Recovery = 80% Analysis Date = 11/24/14 Pct Recovery = 80% Analysis Date = 11/14/14 Pct Recovery = 80% Analysis Date = 11/14/14 Pct Recovery = 80% Analysis Date = 11/05/14 Pct Recovery = 80% Analysis Date = 11/05/14 Pct Recovery = 80% Analysis Date = 10/26/14 Pct Recovery = 79% Analysis Date = 10/26/14 Pct Recovery = 79% Analysis Date = 10/17/14 Pct Recovery = 79% Analysis Date = 10/17/14 Pct Recovery = 79% Analysis Date = 10/08/14 Pct Recovery = 79% Analysis Date = 10/08/14 Pct Recovery = 79% Analysis Date = 09/28/14 Pct Recovery = 79% Analysis Date = 09/28/14 Pct Recovery = 79% Analysis Date = 09/19/14 Pct Recovery = 79% Analysis Date = 09/19/14 Pct Recovery = 79% Analysis Date = 09/09/14 Pct Recovery = 79% Analysis Date = 09/09/14 Pct Recovery = 79% Analysis Date = 08/31/14 Pct Recovery = 78% Analysis Date = 08/31/14 Pct Recovery = 78% Analysis Date = 08/22/14 Pct Recovery = 78% Analysis Date = 08/22/14 Pct Recovery = 78% Analysis Date = 08/12/14 Pct Recovery = 78% Analysis Date = 08/12/14 Pct Recovery = 78% Analysis Date = 08/03/14 Pct Recovery = 78% Analysis Date = 08/03/14 Pct Recovery = 78% Analysis Date = 07/25/14 Pct Recovery = 78% Analysis Date = 07/25/14 Pct Recovery = 78% Analysis Date = 07/15/14 Pct Recovery = 77% Analysis Date = 07/15/14 Pct Recovery = 77% Analysis Date = 07/06/14 Pct Recovery = 77% Analysis Date = 07/06/14 Pct Recovery = 77% Analysis Date = 06/26/14 Pct Recovery = 77% Analysis Date = 06/26/14 Pct Recovery = 77% Analysis Date = 06/17/14 Pct Recovery = 77% Analysis Date = 06/17/14 Pct Recovery = 77% Analysis Date = 06/08/14 Pct Recovery = 77% Analysis Date = 06/08/14 Pct Recovery = 77% Analysis Date = 05/29/14 Pct Recovery = 76% Analysis Date = 05/29/14 Pct Recovery = 76% Analysis Date = 05/20/14 Pct Recovery = 76% Analysis Date = 05/20/14 Pct Recovery = 76% Analysis Date = 05/10/14 Pct Recovery = 76% Analysis Date = 05/10/14 Pct Recovery = 76% Analysis Date = 05/01/14 Pct Recovery = 76% Analysis Date = 05/01/14 Pct Recovery = 76% Analysis Date = 04/22/14 Pct Recovery = 75% Analysis Date = 04/22/14 Pct Recovery = 75% Analysis Date = 04/12/14 Pct Recovery = 75% Analysis Date = 04/12/14 Pct Recovery = 75% Analysis Date = 04/03/14 Pct Recovery = 75% Analysis Date = 04/03/14 Pct Recovery = 75% Analysis Date = 03/24/14 Pct Recovery = 75% Analysis Date = 03/24/14 Pct Recovery = 75% Analysis Date = 03/15/14 Pct Recovery = 75% Analysis Date = 03/15/14 Pct Recovery = 75% Analysis Date = 03/06/14 Pct Recovery = 75% Analysis Date = 03/06/14 Pct Recovery = 75% Analysis Date = 02/24/14 Pct Recovery = 76% Analysis Date = 02/24/14 Pct Recovery = 76% Analysis Date = 02/15/14 Pct Recovery = 76% Analysis Date = 02/15/14 Pct Recovery = 76% Analysis Date = 02/05/14 Pct Recovery = 76% Analysis Date = 02/05/14 Pct Recovery = 76% Analysis Date = 01/27/14 Pct Recovery = 76% Analysis Date = 01/27/14 Pct Recovery = 76% Analysis Date = 01/18/14 Pct Recovery = 76% Analysis Date = 01/18/14 Pct Recovery = 76% Analysis Date = 01/08/14 Pct Recovery = 76% Analysis Date = 01/08/14 Pct Recovery = 76% Analysis Date = 12/30/13 Pct Recovery = 76% Analysis Date = 12/30/13 Pct Recovery = 76% Analysis Date = 12/21/13 Pct Recovery = 77% Analysis Date = 12/21/13 Pct Recovery = 77% Analysis Date = 12/11/13 Pct Recovery = 77% Analysis Date = 12/11/13 Pct Recovery = 77% Analysis Date = 12/02/13 Pct Recovery = 77% Analysis Date = 12/02/13 Pct Recovery = 77% Analysis Date = 11/22/13 Pct Recovery = 78% Analysis Date = 11/22/13 Pct Recovery = 78% Analysis Date = 11/13/13 Pct Recovery = 78% Analysis Date = 11/13/13 Pct Recovery = 78% Analysis Date = 11/04/13 Pct Recovery = 78% Analysis Date = 11/04/13 Pct Recovery = 78% Analysis Date = 10/25/13 Pct Recovery = 79% Analysis Date = 10/25/13 Pct Recovery = 79% Analysis Date = 10/16/13 Pct Recovery = 79% Analysis Date = 10/16/13 Pct Recovery = 79% Analysis Date = 10/06/13 Pct Recovery = 79% Analysis Date = 10/06/13 Pct Recovery = 79% Analysis Date = 09/27/13 Pct Recovery = 80% Analysis Date = 09/27/13 Pct Recovery = 80% Analysis Date = 09/18/13 Pct Recovery = 80% Analysis Date = 09/18/13 Pct Recovery = 80% Analysis Date = 09/08/13 Pct Recovery = 81% Analysis Date = 09/08/13 Pct Recovery = 81% Analysis Date = 08/30/13 Pct Recovery = 81% Analysis Date = 08/30/13 Pct Recovery = 81% Analysis Date = 08/20/13 Pct Recovery = 82% Analysis Date = 08/20/13 Pct Recovery = 82% Analysis Date = 08/11/13 Pct Recovery = 82% Analysis Date = 08/11/13 Pct Recovery = 82% Analysis Date = 08/02/13 Pct Recovery = 82% Analysis Date = 08/02/13 Pct Recovery = 82% Analysis Date = 07/23/13 Pct Recovery = 83% Analysis Date = 07/23/13 Pct Recovery = 83% Analysis Date = 07/14/13 Pct Recovery = 83% Analysis Date = 07/14/13 Pct Recovery = 83% Analysis Date = 07/05/13 Pct Recovery = 84% Analysis Date = 07/05/13 Pct Recovery = 84% Analysis Date = 06/25/13 Pct Recovery = 84% Analysis Date = 06/25/13 Pct Recovery = 84% Analysis Date = 06/16/13 Pct Recovery = 85% Analysis Date = 06/16/13 Pct Recovery = 85% Analysis Date = 06/06/13 Pct Recovery = 85% Analysis Date = 06/06/13 Pct Recovery = 85% Analysis Date = 05/28/13 Pct Recovery = 85% Analysis Date = 05/28/13 Pct Recovery = 85% Analysis Date = 05/19/13 Pct Recovery = 86% Analysis Date = 05/19/13 Pct Recovery = 86% Analysis Date = 05/09/13 Pct Recovery = 86% Analysis Date = 05/09/13 Pct Recovery = 86% Analysis Date = 04/30/13 Pct Recovery = 87% Analysis Date = 04/30/13 Pct Recovery = 87% Analysis Date = 04/20/13 Pct Recovery = 87% Analysis Date = 04/20/13 Pct Recovery = 87% Analysis Date = 04/11/13 Pct Recovery = 88% Analysis Date = 04/11/13 Pct Recovery = 88% Analysis Date = 04/02/13 Pct Recovery = 88% Analysis Date = 04/02/13 Pct Recovery = 88% Analysis Date = 03/23/13 Pct Recovery = 89% Analysis Date = 03/23/13 Pct Recovery = 89% Analysis Date = 03/14/13 Pct Recovery = 89% Analysis Date = 03/14/13 Pct Recovery = 89% Analysis Date = 03/04/13 Pct Recovery = 90% Analysis Date = 03/04/13 Pct Recovery = 90% Analysis Date = 02/23/13 Pct Recovery = 90% Analysis Date = 02/23/13 Pct Recovery = 90% Analysis Date = 02/14/13 Pct Recovery = 91% Analysis Date = 02/14/13 Pct Recovery = 91% Analysis Date = 02/04/13 Pct Recovery = 91% Analysis Date = 02/04/13 Pct Recovery = 91% Analysis Date = 01/26/13 Pct Recovery = 92% Analysis Date = 01/26/13 Pct Recovery = 92% Analysis Date = 01/17/13 Pct Recovery = 92% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
PROPARGITE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 63 82% 21% 81% 17%
Total 63 82% 21% 81% 17%

Sample Statistics
PROPARGITE

Characteristic N % % Basis
Plotted 63 98% Spiked
Estimated Values 14 22% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 64 .  
False Negatives 1 2% 1 out of 64
Not Spiked 38 .  
False Positives 0 0% 0 out of 38

OBSP Determination:
PROPYZAMIDE (PRONAMIDE)
METHOD: 2033 , TESTIDCODE: 82676GCM35

Laboratory ID = 20130250061 Lab Value = 0.272 Expected Conc. = 0.3 Report level label = 0.008 Pct Recovery = 91% Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl SpecificMix = A088380 Laboratory ID = 20140230082 Lab Value = 0.130 Expected Conc. = 0.15 Report level label = 0.008 Pct Recovery = 87% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl SpecificMix = A093651 Laboratory ID = 20132420001 Lab Value = 0.126 Expected Conc. = 0.15 Report level label = 0.008 Pct Recovery = 84% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl SpecificMix = A093651 Laboratory ID = 20130810108 Lab Value = 0.129 Expected Conc. = 0.15 Report level label = 0.008 Pct Recovery = 86% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl SpecificMix = T1120530013 Laboratory ID = 20123560092 Lab Value = 0.128 Expected Conc. = 0.15 Report level label = 0.008 Pct Recovery = 85% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = T1120530013 Laboratory ID = 20140100085 Lab Value = 0.085 Expected Conc. = 0.08 Report level label = 0.008 Pct Recovery = 106% Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl SpecificMix = T1130514013 Laboratory ID = 20132490342 Lab Value = 0.072 Expected Conc. = 0.08 Report level label = 0.008 Pct Recovery = 91% Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl SpecificMix = T1130514013 Laboratory ID = 20140860102 Lab Value = 0.042 Expected Conc. = 0.06 Report level label = 0.008 Pct Recovery = 70% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl SpecificMix = A093651 Laboratory ID = 20133400002 Lab Value = 0.058 Expected Conc. = 0.06 Report level label = 0.008 Pct Recovery = 96% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = A093651 Laboratory ID = 20132910008 Lab Value = 0.049 Expected Conc. = 0.06 Report level label = 0.008 Pct Recovery = 81% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = A093651 Laboratory ID = 20131920149 Lab Value = 0.056 Expected Conc. = 0.06 Report level label = 0.008 Pct Recovery = 94% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl SpecificMix = A093651 Laboratory ID = 20131230084 Lab Value = 0.070 Expected Conc. = 0.06 Report level label = 0.008 Pct Recovery = 117% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl SpecificMix = A088380 Laboratory ID = 20130650005 Lab Value = 0.045 Expected Conc. = 0.06 Report level label = 0.008 Pct Recovery = 74% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl SpecificMix = A088380 Laboratory ID = 20130390105 Lab Value = 0.043 Expected Conc. = 0.06 Report level label = 0.008 Pct Recovery = 72% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl SpecificMix = T1120530013 Laboratory ID = 20172510330 Lab Value = 0.042 Expected Conc. = 0.053 Report level label = 0.008 Pct Recovery = 79% Analysis Date = 12/29/17 SpikeMix = ChemService 6537100: 100 µl & Abs 071817Pest: 100 µl SpecificMix = 6537100 Laboratory ID = 20162860079 Lab Value = 0.045 Expected Conc. = 0.05 Report level label = 0.008 Pct Recovery = 91% Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl SpecificMix = 5054800 Laboratory ID = 20161880109 Lab Value = 0.050 Expected Conc. = 0.05 Report level label = 0.008 Pct Recovery = 101% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl SpecificMix = 5054800 Laboratory ID = 20163370001 Lab Value = 0.041 Expected Conc. = 0.0498 Report level label = 0.008 Pct Recovery = 83% Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl SpecificMix = LC20138V Laboratory ID = 20152610011 Lab Value = 0.035 Expected Conc. = 0.0481 Report level label = 0.008 Pct Recovery = 73% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl SpecificMix = 0406-15-01 Laboratory ID = 20152460215 Lab Value = 0.037 Expected Conc. = 0.0481 Report level label = 0.008 Pct Recovery = 77% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl SpecificMix = 0406-15-01 Laboratory ID = 20171380001 Lab Value = 0.027 Expected Conc. = 0.04 Report level label = 0.008 Pct Recovery = 67% Analysis Date = 06/07/17 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 5054800 Laboratory ID = 20170960001 Lab Value = 0.032 Expected Conc. = 0.04 Report level label = 0.008 Pct Recovery = 79% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl SpecificMix = 5054800 Laboratory ID = 20161740258 Lab Value = 0.025 Expected Conc. = 0.04 Report level label = 0.008 Pct Recovery = 63% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 5054800 Laboratory ID = 20140370077 Lab Value = 0.030 Expected Conc. = 0.04 Report level label = 0.008 Pct Recovery = 76% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl SpecificMix = T1130514013 Laboratory ID = 20132690010 Lab Value = 0.044 Expected Conc. = 0.04 Report level label = 0.008 Pct Recovery = 110% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl SpecificMix = T1130514013 Laboratory ID = 20131370001 Lab Value = 0.047 Expected Conc. = 0.04 Report level label = 0.008 Pct Recovery = 118% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl SpecificMix = 1473000 Laboratory ID = 20171720140 Lab Value = 0.035 Expected Conc. = 0.0398 Report level label = 0.008 Pct Recovery = 89% Analysis Date = 08/31/17 SpikeMix = Supelco LC20138V: 80 µl & Phenova B20160331: 80 µl SpecificMix = LC20138V Laboratory ID = 20170740063 Lab Value = 0.033 Expected Conc. = 0.0398 Report level label = 0.008 Pct Recovery = 83% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl SpecificMix = LC20138V Laboratory ID = 20161470001 Lab Value = 0.033 Expected Conc. = 0.0398 Report level label = 0.008 Pct Recovery = 83% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl SpecificMix = LC20138V Laboratory ID = 20150720069 Lab Value = 0.028 Expected Conc. = 0.0318 Report level label = 0.008 Pct Recovery = 89% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 03DD006 Laboratory ID = 20143110108 Lab Value = 0.021 Expected Conc. = 0.0318 Report level label = 0.008 Pct Recovery = 66% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 03DD006 Laboratory ID = 20142960086 Lab Value = 0.024 Expected Conc. = 0.0318 Report level label = 0.008 Pct Recovery = 76% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 03DD006 Laboratory ID = 20142720002 Lab Value = 0.022 Expected Conc. = 0.0318 Report level label = 0.008 Pct Recovery = 70% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl SpecificMix = LC06435 Laboratory ID = 20142530087 Lab Value = 0.022 Expected Conc. = 0.0318 Report level label = 0.008 Pct Recovery = 68% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl SpecificMix = LC06435 Laboratory ID = 20142270001 Lab Value = 0.021 Expected Conc. = 0.0318 Report level label = 0.008 Pct Recovery = 66% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl SpecificMix = 03DD006 Laboratory ID = 20141570088 Lab Value = 0.029 Expected Conc. = 0.0318 Report level label = 0.008 Pct Recovery = 91% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl SpecificMix = LC06435 Laboratory ID = 20141220025 Lab Value = 0.029 Expected Conc. = 0.0318 Report level label = 0.008 Pct Recovery = 92% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl SpecificMix = LC06435 Laboratory ID = 20172370001 Lab Value = 0.023 Expected Conc. = 0.0265 Report level label = 0.008 Pct Recovery = 87% Analysis Date = 11/18/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6537100: 50 µl SpecificMix = 6537100 Laboratory ID = 20172230001 Lab Value = 0.028 Expected Conc. = 0.0265 Report level label = 0.008 Pct Recovery = 107% Analysis Date = 10/19/17 SpikeMix = ChemService 6472100: 50 µl & Abs 071717Pest: 50 µl SpecificMix = 071717Pest Laboratory ID = 20160770090 Lab Value = 0.016 Expected Conc. = 0.024 Report level label = 0.008 Pct Recovery = 64% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20160630046 Lab Value = 0.014 Expected Conc. = 0.024 Report level label = 0.008 Pct Recovery = 60% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20153510109 Lab Value = 0.017 Expected Conc. = 0.024 Report level label = 0.008 Pct Recovery = 70% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20153440001 Lab Value = 0.017 Expected Conc. = 0.024 Report level label = 0.008 Pct Recovery = 70% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20161260151 Lab Value = 0.017 Expected Conc. = 0.024 Report level label = 0.008 Pct Recovery = 73% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = 3851600 Laboratory ID = 20151550293 Lab Value = 0.024 Expected Conc. = 0.024 Report level label = 0.008 Pct Recovery = 100% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl SpecificMix = 3851600 Laboratory ID = 20151270112 Lab Value = 0.022 Expected Conc. = 0.024 Report level label = 0.008 Pct Recovery = 90% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl SpecificMix = 3851600 Laboratory ID = 20172020035 Lab Value = 0.023 Expected Conc. = 0.0212 Report level label = 0.008 Pct Recovery = 108% Analysis Date = 11/07/17 SpikeMix = Abs 071717Pest: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 071717Pest Laboratory ID = 20171940002 Lab Value = 0.017 Expected Conc. = 0.02 Report level label = 0.008 Pct Recovery = 86% Analysis Date = 11/10/17 SpikeMix = ChemService 5054800: 40 µl & NSI 041816: 40 µl SpecificMix = 5054800 Laboratory ID = 20170460061 Lab Value = 0.017 Expected Conc. = 0.02 Report level label = 0.008 Pct Recovery = 86% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl SpecificMix = 5054800 Laboratory ID = 20163560019 Lab Value = 0.015 Expected Conc. = 0.02 Report level label = 0.008 Pct Recovery = 77% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl SpecificMix = 5054800 Laboratory ID = 20162150213 Lab Value = 0.015 Expected Conc. = 0.02 Report level label = 0.008 Pct Recovery = 77% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl SpecificMix = 5054800 Laboratory ID = 20171510080 Lab Value = 0.018 Expected Conc. = 0.0199 Report level label = 0.008 Pct Recovery = 88% Analysis Date = 06/09/17 SpikeMix = Supelco LC20138V: 40 µl & Crescent 03FF076: 40 µl SpecificMix = LC20138V Laboratory ID = 20162520001 Lab Value = 0.019 Expected Conc. = 0.0199 Report level label = 0.008 Pct Recovery = 95% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl SpecificMix = LC20138V Laboratory ID = 20162660005 Lab Value = 0.014 Expected Conc. = 0.0199 Report level label = 0.008 Pct Recovery = 71% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl SpecificMix = LC20138V Laboratory ID = 20162020124 Lab Value = 0.015 Expected Conc. = 0.0199 Report level label = 0.008 Pct Recovery = 75% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl SpecificMix = LC20138V Laboratory ID = 20140730138 Lab Value = 0.015 Expected Conc. = 0.016 Report level label = 0.008 Pct Recovery = 94% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 1473000 Laboratory ID = 20133470008 Lab Value = 0.016 Expected Conc. = 0.016 Report level label = 0.008 Pct Recovery = 102% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl SpecificMix = 1473000 Laboratory ID = 20133310030 Lab Value = 0.019 Expected Conc. = 0.016 Report level label = 0.008 Pct Recovery = 119% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl SpecificMix = 1473000 Laboratory ID = 20133050050 Lab Value = 0.016 Expected Conc. = 0.016 Report level label = 0.008 Pct Recovery = 103% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl SpecificMix = T1130514013 Laboratory ID = 20132280016 Lab Value = 0.017 Expected Conc. = 0.016 Report level label = 0.008 Pct Recovery = 105% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl SpecificMix = T1130514013 Laboratory ID = 20131790009 Lab Value = 0.018 Expected Conc. = 0.016 Report level label = 0.008 Pct Recovery = 111% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl SpecificMix = 1473000 Laboratory ID = 20131650073 Lab Value = 0.020 Expected Conc. = 0.016 Report level label = 0.008 Pct Recovery = 128% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl SpecificMix = 1473000 Laboratory ID = 20173120093 Lab Value = 0.019 Expected Conc. = 0.0159 Report level label = 0.008 Pct Recovery = 118% Analysis Date = 03/10/18 SpikeMix = ChemService 6472100: 30 µl & ChemService 6537100: 30 µl SpecificMix = 6537100 Laboratory ID = 20172780018 Lab Value = 0.013 Expected Conc. = 0.0159 Report level label = 0.008 Pct Recovery = 84% Analysis Date = 02/08/18 SpikeMix = ChemService 6537100: 30 µl & Abs 071817Pest: 30 µl SpecificMix = 6537100 Laboratory ID = 20150150115 Lab Value = 0.013 Expected Conc. = 0.0159 Report level label = 0.008 Pct Recovery = 84% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl SpecificMix = LC06435 Laboratory ID = 20143370094 Lab Value = 0.011 Expected Conc. = 0.0159 Report level label = 0.008 Pct Recovery = 70% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl SpecificMix = LC06435 Laboratory ID = 20142200164 Lab Value = 0.013 Expected Conc. = 0.0159 Report level label = 0.008 Pct Recovery = 84% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 03DD006 Laboratory ID = 20141910243 Lab Value = 0.010 Expected Conc. = 0.0159 Report level label = 0.008 Pct Recovery = 65% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = LC06435 Laboratory ID = 20141840097 Lab Value = 0.012 Expected Conc. = 0.0159 Report level label = 0.008 Pct Recovery = 74% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl SpecificMix = LC06435 Laboratory ID = 20141640076 Lab Value = 0.013 Expected Conc. = 0.0159 Report level label = 0.008 Pct Recovery = 81% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = 03DD006 Laboratory ID = 20141420140 Lab Value = 0.015 Expected Conc. = 0.0159 Report level label = 0.008 Pct Recovery = 96% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 03DD006 Laboratory ID = 20141080004 Lab Value = 0.013 Expected Conc. = 0.0159 Report level label = 0.008 Pct Recovery = 82% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl SpecificMix = 03DD006 Laboratory ID = 20152190003 Lab Value = 0.009 Expected Conc. = 0.012 Report level label = 0.008 Pct Recovery = 72% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = 0406-15-01 Laboratory ID = 20152040177 Lab Value = 0.010 Expected Conc. = 0.012 Report level label = 0.008 Pct Recovery = 84% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl SpecificMix = 0406-15-01 Laboratory ID = 20160430111 Lab Value = 0.011 Expected Conc. = 0.012 Report level label = 0.008 Pct Recovery = 89% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 3851600 Laboratory ID = 20160210080 Lab Value = 0.008 Expected Conc. = 0.012 Report level label = 0.008 Pct Recovery = 69% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 3851600 Laboratory ID = 20152950078 Lab Value = 0.008 Expected Conc. = 0.012 Report level label = 0.008 Pct Recovery = 66% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 3851600 Laboratory ID = 20153030068 Lab Value = 0.011 Expected Conc. = 0.012 Report level label = 0.008 Pct Recovery = 88% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = 3851600 Laboratory ID = 20151760208 Lab Value = 0.011 Expected Conc. = 0.012 Report level label = 0.008 Pct Recovery = 90% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl SpecificMix = 3851600 Laboratory ID = 20151380009 Lab Value = 0.010 Expected Conc. = 0.012 Report level label = 0.008 Pct Recovery = 85% Analysis Date = 05/30/15 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 3851600 Analysis Date = 03/10/18 Pct Recovery = 93% Analysis Date = 02/28/18 Pct Recovery = 93% Analysis Date = 02/28/18 Pct Recovery = 93% Analysis Date = 02/19/18 Pct Recovery = 93% Analysis Date = 02/19/18 Pct Recovery = 93% Analysis Date = 02/09/18 Pct Recovery = 93% Analysis Date = 02/09/18 Pct Recovery = 93% Analysis Date = 01/31/18 Pct Recovery = 92% Analysis Date = 01/31/18 Pct Recovery = 92% Analysis Date = 01/22/18 Pct Recovery = 92% Analysis Date = 01/22/18 Pct Recovery = 92% Analysis Date = 01/12/18 Pct Recovery = 92% Analysis Date = 01/12/18 Pct Recovery = 92% Analysis Date = 01/03/18 Pct Recovery = 92% Analysis Date = 01/03/18 Pct Recovery = 92% Analysis Date = 12/24/17 Pct Recovery = 91% Analysis Date = 12/24/17 Pct Recovery = 91% Analysis Date = 12/15/17 Pct Recovery = 91% Analysis Date = 12/15/17 Pct Recovery = 91% Analysis Date = 12/06/17 Pct Recovery = 91% Analysis Date = 12/06/17 Pct Recovery = 91% Analysis Date = 11/26/17 Pct Recovery = 91% Analysis Date = 11/26/17 Pct Recovery = 91% Analysis Date = 11/17/17 Pct Recovery = 90% Analysis Date = 11/17/17 Pct Recovery = 90% Analysis Date = 11/07/17 Pct Recovery = 90% Analysis Date = 11/07/17 Pct Recovery = 90% Analysis Date = 10/29/17 Pct Recovery = 90% Analysis Date = 10/29/17 Pct Recovery = 90% Analysis Date = 10/20/17 Pct Recovery = 90% Analysis Date = 10/20/17 Pct Recovery = 90% Analysis Date = 10/10/17 Pct Recovery = 89% Analysis Date = 10/10/17 Pct Recovery = 89% Analysis Date = 10/01/17 Pct Recovery = 89% Analysis Date = 10/01/17 Pct Recovery = 89% Analysis Date = 09/21/17 Pct Recovery = 89% Analysis Date = 09/21/17 Pct Recovery = 89% Analysis Date = 09/12/17 Pct Recovery = 89% Analysis Date = 09/12/17 Pct Recovery = 89% Analysis Date = 09/03/17 Pct Recovery = 89% Analysis Date = 09/03/17 Pct Recovery = 89% Analysis Date = 08/24/17 Pct Recovery = 88% Analysis Date = 08/24/17 Pct Recovery = 88% Analysis Date = 08/15/17 Pct Recovery = 88% Analysis Date = 08/15/17 Pct Recovery = 88% Analysis Date = 08/05/17 Pct Recovery = 88% Analysis Date = 08/05/17 Pct Recovery = 88% Analysis Date = 07/27/17 Pct Recovery = 88% Analysis Date = 07/27/17 Pct Recovery = 88% Analysis Date = 07/18/17 Pct Recovery = 87% Analysis Date = 07/18/17 Pct Recovery = 87% Analysis Date = 07/08/17 Pct Recovery = 87% Analysis Date = 07/08/17 Pct Recovery = 87% Analysis Date = 06/29/17 Pct Recovery = 87% Analysis Date = 06/29/17 Pct Recovery = 87% Analysis Date = 06/19/17 Pct Recovery = 87% Analysis Date = 06/19/17 Pct Recovery = 87% Analysis Date = 06/10/17 Pct Recovery = 86% Analysis Date = 06/10/17 Pct Recovery = 86% Analysis Date = 06/01/17 Pct Recovery = 86% Analysis Date = 06/01/17 Pct Recovery = 86% Analysis Date = 05/22/17 Pct Recovery = 86% Analysis Date = 05/22/17 Pct Recovery = 86% Analysis Date = 05/13/17 Pct Recovery = 86% Analysis Date = 05/13/17 Pct Recovery = 86% Analysis Date = 05/03/17 Pct Recovery = 86% Analysis Date = 05/03/17 Pct Recovery = 86% Analysis Date = 04/24/17 Pct Recovery = 85% Analysis Date = 04/24/17 Pct Recovery = 85% Analysis Date = 04/15/17 Pct Recovery = 85% Analysis Date = 04/15/17 Pct Recovery = 85% Analysis Date = 04/05/17 Pct Recovery = 85% Analysis Date = 04/05/17 Pct Recovery = 85% Analysis Date = 03/27/17 Pct Recovery = 85% Analysis Date = 03/27/17 Pct Recovery = 85% Analysis Date = 03/17/17 Pct Recovery = 85% Analysis Date = 03/17/17 Pct Recovery = 85% Analysis Date = 03/08/17 Pct Recovery = 84% Analysis Date = 03/08/17 Pct Recovery = 84% Analysis Date = 02/27/17 Pct Recovery = 84% Analysis Date = 02/27/17 Pct Recovery = 84% Analysis Date = 02/17/17 Pct Recovery = 84% Analysis Date = 02/17/17 Pct Recovery = 84% Analysis Date = 02/08/17 Pct Recovery = 84% Analysis Date = 02/08/17 Pct Recovery = 84% Analysis Date = 01/29/17 Pct Recovery = 83% Analysis Date = 01/29/17 Pct Recovery = 83% Analysis Date = 01/20/17 Pct Recovery = 83% Analysis Date = 01/20/17 Pct Recovery = 83% Analysis Date = 01/11/17 Pct Recovery = 83% Analysis Date = 01/11/17 Pct Recovery = 83% Analysis Date = 01/01/17 Pct Recovery = 83% Analysis Date = 01/01/17 Pct Recovery = 83% Analysis Date = 12/23/16 Pct Recovery = 83% Analysis Date = 12/23/16 Pct Recovery = 83% Analysis Date = 12/13/16 Pct Recovery = 83% Analysis Date = 12/13/16 Pct Recovery = 83% Analysis Date = 12/04/16 Pct Recovery = 82% Analysis Date = 12/04/16 Pct Recovery = 82% Analysis Date = 11/25/16 Pct Recovery = 82% Analysis Date = 11/25/16 Pct Recovery = 82% Analysis Date = 11/15/16 Pct Recovery = 82% Analysis Date = 11/15/16 Pct Recovery = 82% Analysis Date = 11/06/16 Pct Recovery = 82% Analysis Date = 11/06/16 Pct Recovery = 82% Analysis Date = 10/27/16 Pct Recovery = 82% Analysis Date = 10/27/16 Pct Recovery = 82% Analysis Date = 10/18/16 Pct Recovery = 81% Analysis Date = 10/18/16 Pct Recovery = 81% Analysis Date = 10/09/16 Pct Recovery = 81% Analysis Date = 10/09/16 Pct Recovery = 81% Analysis Date = 09/29/16 Pct Recovery = 81% Analysis Date = 09/29/16 Pct Recovery = 81% Analysis Date = 09/20/16 Pct Recovery = 81% Analysis Date = 09/20/16 Pct Recovery = 81% Analysis Date = 09/10/16 Pct Recovery = 81% Analysis Date = 09/10/16 Pct Recovery = 81% Analysis Date = 09/01/16 Pct Recovery = 80% Analysis Date = 09/01/16 Pct Recovery = 80% Analysis Date = 08/23/16 Pct Recovery = 80% Analysis Date = 08/23/16 Pct Recovery = 80% Analysis Date = 08/13/16 Pct Recovery = 80% Analysis Date = 08/13/16 Pct Recovery = 80% Analysis Date = 08/04/16 Pct Recovery = 80% Analysis Date = 08/04/16 Pct Recovery = 80% Analysis Date = 07/25/16 Pct Recovery = 80% Analysis Date = 07/25/16 Pct Recovery = 80% Analysis Date = 07/16/16 Pct Recovery = 80% Analysis Date = 07/16/16 Pct Recovery = 80% Analysis Date = 07/07/16 Pct Recovery = 80% Analysis Date = 07/07/16 Pct Recovery = 80% Analysis Date = 06/27/16 Pct Recovery = 80% Analysis Date = 06/27/16 Pct Recovery = 80% Analysis Date = 06/18/16 Pct Recovery = 79% Analysis Date = 06/18/16 Pct Recovery = 79% Analysis Date = 06/08/16 Pct Recovery = 79% Analysis Date = 06/08/16 Pct Recovery = 79% Analysis Date = 05/30/16 Pct Recovery = 79% Analysis Date = 05/30/16 Pct Recovery = 79% Analysis Date = 05/21/16 Pct Recovery = 79% Analysis Date = 05/21/16 Pct Recovery = 79% Analysis Date = 05/11/16 Pct Recovery = 79% Analysis Date = 05/11/16 Pct Recovery = 79% Analysis Date = 05/02/16 Pct Recovery = 79% Analysis Date = 05/02/16 Pct Recovery = 79% Analysis Date = 04/22/16 Pct Recovery = 79% Analysis Date = 04/22/16 Pct Recovery = 79% Analysis Date = 04/13/16 Pct Recovery = 79% Analysis Date = 04/13/16 Pct Recovery = 79% Analysis Date = 04/04/16 Pct Recovery = 79% Analysis Date = 04/04/16 Pct Recovery = 79% Analysis Date = 03/25/16 Pct Recovery = 79% Analysis Date = 03/25/16 Pct Recovery = 79% Analysis Date = 03/16/16 Pct Recovery = 78% Analysis Date = 03/16/16 Pct Recovery = 78% Analysis Date = 03/06/16 Pct Recovery = 78% Analysis Date = 03/06/16 Pct Recovery = 78% Analysis Date = 02/26/16 Pct Recovery = 78% Analysis Date = 02/26/16 Pct Recovery = 78% Analysis Date = 02/17/16 Pct Recovery = 78% Analysis Date = 02/17/16 Pct Recovery = 78% Analysis Date = 02/07/16 Pct Recovery = 78% Analysis Date = 02/07/16 Pct Recovery = 78% Analysis Date = 01/29/16 Pct Recovery = 78% Analysis Date = 01/29/16 Pct Recovery = 78% Analysis Date = 01/19/16 Pct Recovery = 78% Analysis Date = 01/19/16 Pct Recovery = 78% Analysis Date = 01/10/16 Pct Recovery = 78% Analysis Date = 01/10/16 Pct Recovery = 78% Analysis Date = 01/01/16 Pct Recovery = 78% Analysis Date = 01/01/16 Pct Recovery = 78% Analysis Date = 12/22/15 Pct Recovery = 78% Analysis Date = 12/22/15 Pct Recovery = 78% Analysis Date = 12/13/15 Pct Recovery = 78% Analysis Date = 12/13/15 Pct Recovery = 78% Analysis Date = 12/03/15 Pct Recovery = 78% Analysis Date = 12/03/15 Pct Recovery = 78% Analysis Date = 11/24/15 Pct Recovery = 78% Analysis Date = 11/24/15 Pct Recovery = 78% Analysis Date = 11/15/15 Pct Recovery = 78% Analysis Date = 11/15/15 Pct Recovery = 78% Analysis Date = 11/05/15 Pct Recovery = 78% Analysis Date = 11/05/15 Pct Recovery = 78% Analysis Date = 10/27/15 Pct Recovery = 78% Analysis Date = 10/27/15 Pct Recovery = 78% Analysis Date = 10/17/15 Pct Recovery = 78% Analysis Date = 10/17/15 Pct Recovery = 78% Analysis Date = 10/08/15 Pct Recovery = 78% Analysis Date = 10/08/15 Pct Recovery = 78% Analysis Date = 09/29/15 Pct Recovery = 78% Analysis Date = 09/29/15 Pct Recovery = 78% Analysis Date = 09/19/15 Pct Recovery = 78% Analysis Date = 09/19/15 Pct Recovery = 78% Analysis Date = 09/10/15 Pct Recovery = 78% Analysis Date = 09/10/15 Pct Recovery = 78% Analysis Date = 08/31/15 Pct Recovery = 78% Analysis Date = 08/31/15 Pct Recovery = 78% Analysis Date = 08/22/15 Pct Recovery = 78% Analysis Date = 08/22/15 Pct Recovery = 78% Analysis Date = 08/13/15 Pct Recovery = 78% Analysis Date = 08/13/15 Pct Recovery = 78% Analysis Date = 08/03/15 Pct Recovery = 78% Analysis Date = 08/03/15 Pct Recovery = 78% Analysis Date = 07/25/15 Pct Recovery = 78% Analysis Date = 07/25/15 Pct Recovery = 78% Analysis Date = 07/15/15 Pct Recovery = 78% Analysis Date = 07/15/15 Pct Recovery = 78% Analysis Date = 07/06/15 Pct Recovery = 78% Analysis Date = 07/06/15 Pct Recovery = 78% Analysis Date = 06/27/15 Pct Recovery = 78% Analysis Date = 06/27/15 Pct Recovery = 78% Analysis Date = 06/17/15 Pct Recovery = 78% Analysis Date = 06/17/15 Pct Recovery = 78% Analysis Date = 06/08/15 Pct Recovery = 78% Analysis Date = 06/08/15 Pct Recovery = 78% Analysis Date = 05/29/15 Pct Recovery = 78% Analysis Date = 05/29/15 Pct Recovery = 78% Analysis Date = 05/20/15 Pct Recovery = 79% Analysis Date = 05/20/15 Pct Recovery = 79% Analysis Date = 05/11/15 Pct Recovery = 79% Analysis Date = 05/11/15 Pct Recovery = 79% Analysis Date = 05/01/15 Pct Recovery = 79% Analysis Date = 05/01/15 Pct Recovery = 79% Analysis Date = 04/22/15 Pct Recovery = 79% Analysis Date = 04/22/15 Pct Recovery = 79% Analysis Date = 04/12/15 Pct Recovery = 79% Analysis Date = 04/12/15 Pct Recovery = 79% Analysis Date = 04/03/15 Pct Recovery = 79% Analysis Date = 04/03/15 Pct Recovery = 79% Analysis Date = 03/25/15 Pct Recovery = 79% Analysis Date = 03/25/15 Pct Recovery = 79% Analysis Date = 03/15/15 Pct Recovery = 79% Analysis Date = 03/15/15 Pct Recovery = 79% Analysis Date = 03/06/15 Pct Recovery = 79% Analysis Date = 03/06/15 Pct Recovery = 79% Analysis Date = 02/24/15 Pct Recovery = 80% Analysis Date = 02/24/15 Pct Recovery = 80% Analysis Date = 02/15/15 Pct Recovery = 80% Analysis Date = 02/15/15 Pct Recovery = 80% Analysis Date = 02/06/15 Pct Recovery = 80% Analysis Date = 02/06/15 Pct Recovery = 80% Analysis Date = 01/27/15 Pct Recovery = 80% Analysis Date = 01/27/15 Pct Recovery = 80% Analysis Date = 01/18/15 Pct Recovery = 80% Analysis Date = 01/18/15 Pct Recovery = 80% Analysis Date = 01/08/15 Pct Recovery = 81% Analysis Date = 01/08/15 Pct Recovery = 81% Analysis Date = 12/30/14 Pct Recovery = 81% Analysis Date = 12/30/14 Pct Recovery = 81% Analysis Date = 12/21/14 Pct Recovery = 81% Analysis Date = 12/21/14 Pct Recovery = 81% Analysis Date = 12/11/14 Pct Recovery = 81% Analysis Date = 12/11/14 Pct Recovery = 81% Analysis Date = 12/02/14 Pct Recovery = 81% Analysis Date = 12/02/14 Pct Recovery = 81% Analysis Date = 11/22/14 Pct Recovery = 81% Analysis Date = 11/22/14 Pct Recovery = 81% Analysis Date = 11/13/14 Pct Recovery = 82% Analysis Date = 11/13/14 Pct Recovery = 82% Analysis Date = 11/04/14 Pct Recovery = 82% Analysis Date = 11/04/14 Pct Recovery = 82% Analysis Date = 10/25/14 Pct Recovery = 82% Analysis Date = 10/25/14 Pct Recovery = 82% Analysis Date = 10/16/14 Pct Recovery = 82% Analysis Date = 10/16/14 Pct Recovery = 82% Analysis Date = 10/06/14 Pct Recovery = 82% Analysis Date = 10/06/14 Pct Recovery = 82% Analysis Date = 09/27/14 Pct Recovery = 83% Analysis Date = 09/27/14 Pct Recovery = 83% Analysis Date = 09/18/14 Pct Recovery = 83% Analysis Date = 09/18/14 Pct Recovery = 83% Analysis Date = 09/08/14 Pct Recovery = 83% Analysis Date = 09/08/14 Pct Recovery = 83% Analysis Date = 08/30/14 Pct Recovery = 83% Analysis Date = 08/30/14 Pct Recovery = 83% Analysis Date = 08/20/14 Pct Recovery = 84% Analysis Date = 08/20/14 Pct Recovery = 84% Analysis Date = 08/11/14 Pct Recovery = 84% Analysis Date = 08/11/14 Pct Recovery = 84% Analysis Date = 08/02/14 Pct Recovery = 84% Analysis Date = 08/02/14 Pct Recovery = 84% Analysis Date = 07/23/14 Pct Recovery = 85% Analysis Date = 07/23/14 Pct Recovery = 85% Analysis Date = 07/14/14 Pct Recovery = 85% Analysis Date = 07/14/14 Pct Recovery = 85% Analysis Date = 07/04/14 Pct Recovery = 85% Analysis Date = 07/04/14 Pct Recovery = 85% Analysis Date = 06/25/14 Pct Recovery = 85% Analysis Date = 06/25/14 Pct Recovery = 85% Analysis Date = 06/16/14 Pct Recovery = 85% Analysis Date = 06/16/14 Pct Recovery = 85% Analysis Date = 06/06/14 Pct Recovery = 86% Analysis Date = 06/06/14 Pct Recovery = 86% Analysis Date = 05/28/14 Pct Recovery = 86% Analysis Date = 05/28/14 Pct Recovery = 86% Analysis Date = 05/18/14 Pct Recovery = 86% Analysis Date = 05/18/14 Pct Recovery = 86% Analysis Date = 05/09/14 Pct Recovery = 86% Analysis Date = 05/09/14 Pct Recovery = 86% Analysis Date = 04/30/14 Pct Recovery = 87% Analysis Date = 04/30/14 Pct Recovery = 87% Analysis Date = 04/20/14 Pct Recovery = 87% Analysis Date = 04/20/14 Pct Recovery = 87% Analysis Date = 04/11/14 Pct Recovery = 87% Analysis Date = 04/11/14 Pct Recovery = 87% Analysis Date = 04/01/14 Pct Recovery = 88% Analysis Date = 04/01/14 Pct Recovery = 88% Analysis Date = 03/23/14 Pct Recovery = 88% Analysis Date = 03/23/14 Pct Recovery = 88% Analysis Date = 03/14/14 Pct Recovery = 88% Analysis Date = 03/14/14 Pct Recovery = 88% Analysis Date = 03/04/14 Pct Recovery = 89% Analysis Date = 03/04/14 Pct Recovery = 89% Analysis Date = 02/23/14 Pct Recovery = 89% Analysis Date = 02/23/14 Pct Recovery = 89% Analysis Date = 02/13/14 Pct Recovery = 89% Analysis Date = 02/13/14 Pct Recovery = 89% Analysis Date = 02/04/14 Pct Recovery = 90% Analysis Date = 02/04/14 Pct Recovery = 90% Analysis Date = 01/26/14 Pct Recovery = 90% Analysis Date = 01/26/14 Pct Recovery = 90% Analysis Date = 01/16/14 Pct Recovery = 90% Analysis Date = 01/16/14 Pct Recovery = 90% Analysis Date = 01/07/14 Pct Recovery = 91% Analysis Date = 01/07/14 Pct Recovery = 91% Analysis Date = 12/28/13 Pct Recovery = 91% Analysis Date = 12/28/13 Pct Recovery = 91% Analysis Date = 12/19/13 Pct Recovery = 91% Analysis Date = 12/19/13 Pct Recovery = 91% Analysis Date = 12/10/13 Pct Recovery = 91% Analysis Date = 12/10/13 Pct Recovery = 91% Analysis Date = 11/30/13 Pct Recovery = 92% Analysis Date = 11/30/13 Pct Recovery = 92% Analysis Date = 11/21/13 Pct Recovery = 92% Analysis Date = 11/21/13 Pct Recovery = 92% Analysis Date = 11/11/13 Pct Recovery = 92% Analysis Date = 11/11/13 Pct Recovery = 92% Analysis Date = 11/02/13 Pct Recovery = 93% Analysis Date = 11/02/13 Pct Recovery = 93% Analysis Date = 10/24/13 Pct Recovery = 93% Analysis Date = 10/24/13 Pct Recovery = 93% Analysis Date = 10/14/13 Pct Recovery = 93% Analysis Date = 10/14/13 Pct Recovery = 93% Analysis Date = 10/05/13 Pct Recovery = 93% Analysis Date = 10/05/13 Pct Recovery = 93% Analysis Date = 09/25/13 Pct Recovery = 94% Analysis Date = 09/25/13 Pct Recovery = 94% Analysis Date = 09/16/13 Pct Recovery = 94% Analysis Date = 09/16/13 Pct Recovery = 94% Analysis Date = 09/07/13 Pct Recovery = 94% Analysis Date = 09/07/13 Pct Recovery = 94% Analysis Date = 08/28/13 Pct Recovery = 95% Analysis Date = 08/28/13 Pct Recovery = 95% Analysis Date = 08/19/13 Pct Recovery = 95% Analysis Date = 08/19/13 Pct Recovery = 95% Analysis Date = 08/09/13 Pct Recovery = 95% Analysis Date = 08/09/13 Pct Recovery = 95% Analysis Date = 07/31/13 Pct Recovery = 95% Analysis Date = 07/31/13 Pct Recovery = 95% Analysis Date = 07/22/13 Pct Recovery = 96% Analysis Date = 07/22/13 Pct Recovery = 96% Analysis Date = 07/12/13 Pct Recovery = 96% Analysis Date = 07/12/13 Pct Recovery = 96% Analysis Date = 07/03/13 Pct Recovery = 96% Analysis Date = 07/03/13 Pct Recovery = 96% Analysis Date = 06/23/13 Pct Recovery = 97% Analysis Date = 06/23/13 Pct Recovery = 97% Analysis Date = 06/14/13 Pct Recovery = 97% Analysis Date = 06/14/13 Pct Recovery = 97% Analysis Date = 06/05/13 Pct Recovery = 97% Analysis Date = 06/05/13 Pct Recovery = 97% Analysis Date = 05/26/13 Pct Recovery = 97% Analysis Date = 05/26/13 Pct Recovery = 97% Analysis Date = 05/17/13 Pct Recovery = 98% Analysis Date = 05/17/13 Pct Recovery = 98% Analysis Date = 05/07/13 Pct Recovery = 98% Analysis Date = 05/07/13 Pct Recovery = 98% Analysis Date = 04/28/13 Pct Recovery = 98% Analysis Date = 04/28/13 Pct Recovery = 98% Analysis Date = 04/19/13 Pct Recovery = 99% Analysis Date = 04/19/13 Pct Recovery = 99% Analysis Date = 04/09/13 Pct Recovery = 99% Analysis Date = 04/09/13 Pct Recovery = 99% Analysis Date = 03/31/13 Pct Recovery = 99% Analysis Date = 03/31/13 Pct Recovery = 99% Analysis Date = 03/21/13 Pct Recovery = 99% Analysis Date = 03/21/13 Pct Recovery = 99% Analysis Date = 03/12/13 Pct Recovery = 100% Analysis Date = 03/12/13 Pct Recovery = 100% Analysis Date = 03/03/13 Pct Recovery = 100% Analysis Date = 03/03/13 Pct Recovery = 100% Analysis Date = 02/21/13 Pct Recovery = 100% Analysis Date = 02/21/13 Pct Recovery = 100% Analysis Date = 02/12/13 Pct Recovery = 100% Analysis Date = 02/12/13 Pct Recovery = 100% Analysis Date = 02/02/13 Pct Recovery = 101% Analysis Date = 02/02/13 Pct Recovery = 101% Analysis Date = 01/24/13 Pct Recovery = 101% Analysis Date = 01/24/13 Pct Recovery = 101% Analysis Date = 01/15/13 Pct Recovery = 101% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
PROPYZAMIDE (PRONAMIDE)

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 80 86% 15% 84% 14%
Total 80 86% 15% 84% 14%

Sample Statistics
PROPYZAMIDE (PRONAMIDE)

Characteristic N % % Basis
Plotted 80 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 80 .  
False Negatives 0 0% 0 out of 80
Not Spiked 38 .  
False Positives 0 0% 0 out of 38

OBSP Determination:
SIMAZINE
METHOD: 2033 , TESTIDCODE: 04035GCM35

Laboratory ID = 20140100085 Lab Value = 0.105 Expected Conc. = 0.1 Report level label = 0.006 Pct Recovery = 105% Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl SpecificMix = T1130514013 Laboratory ID = 20132490342 Lab Value = 0.093 Expected Conc. = 0.1 Report level label = 0.006 Pct Recovery = 93% Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl SpecificMix = T1130514013 Laboratory ID = 20130250061 Lab Value = 0.090 Expected Conc. = 0.1 Report level label = 0.006 Pct Recovery = 90% Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl SpecificMix = A088380 Laboratory ID = 20140370077 Lab Value = 0.032 Expected Conc. = 0.05 Report level label = 0.006 Pct Recovery = 64% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl SpecificMix = T1130514013 Laboratory ID = 20140230082 Lab Value = 0.044 Expected Conc. = 0.05 Report level label = 0.006 Pct Recovery = 88% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl SpecificMix = A093651 Laboratory ID = 20132690010 Lab Value = 0.057 Expected Conc. = 0.05 Report level label = 0.006 Pct Recovery = 113% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl SpecificMix = T1130514013 Laboratory ID = 20132420001 Lab Value = 0.046 Expected Conc. = 0.05 Report level label = 0.006 Pct Recovery = 92% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl SpecificMix = A093651 Laboratory ID = 20131370001 Lab Value = 0.047 Expected Conc. = 0.05 Report level label = 0.006 Pct Recovery = 95% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl SpecificMix = 1473000 Laboratory ID = 20130810108 Lab Value = 0.035 Expected Conc. = 0.05 Report level label = 0.006 Pct Recovery = 71% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl SpecificMix = T1120530013 Laboratory ID = 20123560092 Lab Value = 0.033 Expected Conc. = 0.05 Report level label = 0.006 Pct Recovery = 67% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = T1120530013 Laboratory ID = 20162860079 Lab Value = 0.049 Expected Conc. = 0.04 Report level label = 0.006 Pct Recovery = 121% Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl SpecificMix = 5054800 Laboratory ID = 20161880109 Lab Value = 0.044 Expected Conc. = 0.04 Report level label = 0.006 Pct Recovery = 111% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl SpecificMix = 5054800 Laboratory ID = 20163370001 Lab Value = 0.038 Expected Conc. = 0.0375 Report level label = 0.006 Pct Recovery = 100% Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl SpecificMix = LC20138V Laboratory ID = 20152750006 Lab Value = 0.034 Expected Conc. = 0.036 Report level label = 0.006 Pct Recovery = 96% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl SpecificMix = EN150514012 Laboratory ID = 20152460215 Lab Value = 0.030 Expected Conc. = 0.036 Report level label = 0.006 Pct Recovery = 84% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl SpecificMix = EN150514012 Laboratory ID = 20171380001 Lab Value = 0.029 Expected Conc. = 0.032 Report level label = 0.006 Pct Recovery = 92% Analysis Date = 06/07/17 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 5054800 Laboratory ID = 20170960001 Lab Value = 0.028 Expected Conc. = 0.032 Report level label = 0.006 Pct Recovery = 87% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl SpecificMix = 5054800 Laboratory ID = 20161740258 Lab Value = 0.027 Expected Conc. = 0.032 Report level label = 0.006 Pct Recovery = 84% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 5054800 Laboratory ID = 20171720140 Lab Value = 0.027 Expected Conc. = 0.03 Report level label = 0.006 Pct Recovery = 88% Analysis Date = 08/31/17 SpikeMix = Supelco LC20138V: 80 µl & Phenova B20160331: 80 µl SpecificMix = LC20138V Laboratory ID = 20170740063 Lab Value = 0.018 Expected Conc. = 0.03 Report level label = 0.006 Pct Recovery = 59% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl SpecificMix = LC20138V Laboratory ID = 20161470001 Lab Value = 0.030 Expected Conc. = 0.03 Report level label = 0.006 Pct Recovery = 99% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl SpecificMix = LC20138V Laboratory ID = 20142720002 Lab Value = 0.017 Expected Conc. = 0.0241 Report level label = 0.006 Pct Recovery = 70% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl SpecificMix = LC06435 Laboratory ID = 20142530087 Lab Value = 0.021 Expected Conc. = 0.0241 Report level label = 0.006 Pct Recovery = 85% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl SpecificMix = LC06435 Laboratory ID = 20141570088 Lab Value = 0.028 Expected Conc. = 0.0241 Report level label = 0.006 Pct Recovery = 117% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl SpecificMix = LC06435 Laboratory ID = 20141220025 Lab Value = 0.022 Expected Conc. = 0.0241 Report level label = 0.006 Pct Recovery = 90% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl SpecificMix = LC06435 Laboratory ID = 20150720069 Lab Value = 0.016 Expected Conc. = 0.024 Report level label = 0.006 Pct Recovery = 68% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 03DD006 Laboratory ID = 20143110108 Lab Value = 0.019 Expected Conc. = 0.024 Report level label = 0.006 Pct Recovery = 78% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 03DD006 Laboratory ID = 20142960086 Lab Value = 0.024 Expected Conc. = 0.024 Report level label = 0.006 Pct Recovery = 98% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 03DD006 Laboratory ID = 20142270001 Lab Value = 0.017 Expected Conc. = 0.024 Report level label = 0.006 Pct Recovery = 72% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl SpecificMix = 03DD006 Laboratory ID = 20172560101 Lab Value = 0.017 Expected Conc. = 0.0203 Report level label = 0.006 Pct Recovery = 86% Analysis Date = 12/22/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6567600: 50 µl SpecificMix = EN170808006 Laboratory ID = 20172370001 Lab Value = 0.022 Expected Conc. = 0.0203 Report level label = 0.006 Pct Recovery = 108% Analysis Date = 11/18/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6537100: 50 µl SpecificMix = EN170808006 Laboratory ID = 20172230001 Lab Value = 0.026 Expected Conc. = 0.02 Report level label = 0.006 Pct Recovery = 130% Analysis Date = 10/19/17 SpikeMix = ChemService 6472100: 50 µl & Abs 071717Pest: 50 µl SpecificMix = 6472100 Laboratory ID = 20140860102 Lab Value = 0.016 Expected Conc. = 0.02 Report level label = 0.006 Pct Recovery = 80% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl SpecificMix = A093651 Laboratory ID = 20140730138 Lab Value = 0.013 Expected Conc. = 0.02 Report level label = 0.006 Pct Recovery = 65% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 1473000 Laboratory ID = 20133400002 Lab Value = 0.020 Expected Conc. = 0.02 Report level label = 0.006 Pct Recovery = 100% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = A093651 Laboratory ID = 20133470008 Lab Value = 0.019 Expected Conc. = 0.02 Report level label = 0.006 Pct Recovery = 94% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl SpecificMix = 1473000 Laboratory ID = 20133310030 Lab Value = 0.020 Expected Conc. = 0.02 Report level label = 0.006 Pct Recovery = 100% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl SpecificMix = 1473000 Laboratory ID = 20133050050 Lab Value = 0.019 Expected Conc. = 0.02 Report level label = 0.006 Pct Recovery = 95% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl SpecificMix = T1130514013 Laboratory ID = 20132910008 Lab Value = 0.017 Expected Conc. = 0.02 Report level label = 0.006 Pct Recovery = 86% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = A093651 Laboratory ID = 20132280016 Lab Value = 0.021 Expected Conc. = 0.02 Report level label = 0.006 Pct Recovery = 103% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl SpecificMix = T1130514013 Laboratory ID = 20131920149 Lab Value = 0.019 Expected Conc. = 0.02 Report level label = 0.006 Pct Recovery = 97% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl SpecificMix = A093651 Laboratory ID = 20131790009 Lab Value = 0.021 Expected Conc. = 0.02 Report level label = 0.006 Pct Recovery = 106% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl SpecificMix = 1473000 Laboratory ID = 20131650073 Lab Value = 0.024 Expected Conc. = 0.02 Report level label = 0.006 Pct Recovery = 121% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl SpecificMix = 1473000 Laboratory ID = 20131230084 Lab Value = 0.024 Expected Conc. = 0.02 Report level label = 0.006 Pct Recovery = 119% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl SpecificMix = A088380 Laboratory ID = 20130650005 Lab Value = 0.015 Expected Conc. = 0.02 Report level label = 0.006 Pct Recovery = 76% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl SpecificMix = A088380 Laboratory ID = 20130390105 Lab Value = 0.013 Expected Conc. = 0.02 Report level label = 0.006 Pct Recovery = 65% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl SpecificMix = T1120530013 Laboratory ID = 20160630046 Lab Value = 0.014 Expected Conc. = 0.018 Report level label = 0.006 Pct Recovery = 75% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = EN150514012 Laboratory ID = 20153440001 Lab Value = 0.013 Expected Conc. = 0.018 Report level label = 0.006 Pct Recovery = 74% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = EN150514012 Laboratory ID = 20152330039 Lab Value = 0.017 Expected Conc. = 0.018 Report level label = 0.006 Pct Recovery = 94% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl SpecificMix = 041415 Laboratory ID = 20151900132 Lab Value = 0.019 Expected Conc. = 0.018 Report level label = 0.006 Pct Recovery = 104% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl SpecificMix = 041415 Laboratory ID = 20151270112 Lab Value = 0.016 Expected Conc. = 0.018 Report level label = 0.006 Pct Recovery = 87% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl SpecificMix = 041415 Laboratory ID = 20171940002 Lab Value = 0.019 Expected Conc. = 0.016 Report level label = 0.006 Pct Recovery = 116% Analysis Date = 11/10/17 SpikeMix = ChemService 5054800: 40 µl & NSI 041816: 40 µl SpecificMix = 5054800 Laboratory ID = 20170460061 Lab Value = 0.014 Expected Conc. = 0.016 Report level label = 0.006 Pct Recovery = 89% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl SpecificMix = 5054800 Laboratory ID = 20163560019 Lab Value = 0.014 Expected Conc. = 0.016 Report level label = 0.006 Pct Recovery = 90% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl SpecificMix = 5054800 Laboratory ID = 20162150213 Lab Value = 0.014 Expected Conc. = 0.016 Report level label = 0.006 Pct Recovery = 86% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl SpecificMix = 5054800 Laboratory ID = 20171510080 Lab Value = 0.017 Expected Conc. = 0.015 Report level label = 0.006 Pct Recovery = 110% Analysis Date = 06/09/17 SpikeMix = Supelco LC20138V: 40 µl & Crescent 03FF076: 40 µl SpecificMix = LC20138V Laboratory ID = 20162520001 Lab Value = 0.021 Expected Conc. = 0.015 Report level label = 0.006 Pct Recovery = 141% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl SpecificMix = LC20138V Laboratory ID = 20162660005 Lab Value = 0.014 Expected Conc. = 0.015 Report level label = 0.006 Pct Recovery = 90% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl SpecificMix = LC20138V Laboratory ID = 20162020124 Lab Value = 0.018 Expected Conc. = 0.015 Report level label = 0.006 Pct Recovery = 118% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl SpecificMix = LC20138V Laboratory ID = 20150150115 Lab Value = 0.010 Expected Conc. = 0.0121 Report level label = 0.006 Pct Recovery = 85% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl SpecificMix = LC06435 Laboratory ID = 20143370094 Lab Value = 0.010 Expected Conc. = 0.0121 Report level label = 0.006 Pct Recovery = 85% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl SpecificMix = LC06435 Laboratory ID = 20141910243 Lab Value = 0.010 Expected Conc. = 0.0121 Report level label = 0.006 Pct Recovery = 81% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = LC06435 Laboratory ID = 20141840097 Lab Value = 0.011 Expected Conc. = 0.0121 Report level label = 0.006 Pct Recovery = 91% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl SpecificMix = LC06435 Laboratory ID = 20173120093 Lab Value = 0.017 Expected Conc. = 0.012 Report level label = 0.006 Pct Recovery = 140% Analysis Date = 03/10/18 SpikeMix = ChemService 6472100: 30 µl & ChemService 6537100: 30 µl SpecificMix = 6472100 Laboratory ID = 20142200164 Lab Value = 0.013 Expected Conc. = 0.012 Report level label = 0.006 Pct Recovery = 108% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 03DD006 Laboratory ID = 20141640076 Lab Value = 0.011 Expected Conc. = 0.012 Report level label = 0.006 Pct Recovery = 95% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = 03DD006 Laboratory ID = 20141420140 Lab Value = 0.012 Expected Conc. = 0.012 Report level label = 0.006 Pct Recovery = 96% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 03DD006 Laboratory ID = 20141080004 Lab Value = 0.011 Expected Conc. = 0.012 Report level label = 0.006 Pct Recovery = 93% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl SpecificMix = 03DD006 Laboratory ID = 20161050143 Lab Value = 0.011 Expected Conc. = 0.009 Report level label = 0.006 Pct Recovery = 118% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 041415 Laboratory ID = 20160560044 Lab Value = 0.009 Expected Conc. = 0.009 Report level label = 0.006 Pct Recovery = 100% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl SpecificMix = 041415 Laboratory ID = 20160210080 Lab Value = 0.008 Expected Conc. = 0.009 Report level label = 0.006 Pct Recovery = 90% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 041415 Laboratory ID = 20160070059 Lab Value = 0.009 Expected Conc. = 0.009 Report level label = 0.006 Pct Recovery = 99% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = EN150514012 Laboratory ID = 20153160001 Lab Value = 0.009 Expected Conc. = 0.009 Report level label = 0.006 Pct Recovery = 101% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = EN150514012 Laboratory ID = 20152950078 Lab Value = 0.007 Expected Conc. = 0.009 Report level label = 0.006 Pct Recovery = 76% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 041415 Laboratory ID = 20152040177 Lab Value = 0.008 Expected Conc. = 0.009 Report level label = 0.006 Pct Recovery = 93% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl SpecificMix = 041415 Laboratory ID = 20151760208 Lab Value = 0.008 Expected Conc. = 0.009 Report level label = 0.006 Pct Recovery = 92% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl SpecificMix = EN150514012 Laboratory ID = 20151480170 Lab Value = 0.008 Expected Conc. = 0.009 Report level label = 0.006 Pct Recovery = 92% Analysis Date = 06/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150514012 Laboratory ID = 20151210037 Lab Value = 0.010 Expected Conc. = 0.009 Report level label = 0.006 Pct Recovery = 113% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 041415 Analysis Date = 03/10/18 Pct Recovery = 110% Analysis Date = 02/28/18 Pct Recovery = 110% Analysis Date = 02/28/18 Pct Recovery = 110% Analysis Date = 02/19/18 Pct Recovery = 110% Analysis Date = 02/19/18 Pct Recovery = 110% Analysis Date = 02/09/18 Pct Recovery = 110% Analysis Date = 02/09/18 Pct Recovery = 110% Analysis Date = 01/31/18 Pct Recovery = 109% Analysis Date = 01/31/18 Pct Recovery = 109% Analysis Date = 01/22/18 Pct Recovery = 109% Analysis Date = 01/22/18 Pct Recovery = 109% Analysis Date = 01/12/18 Pct Recovery = 109% Analysis Date = 01/12/18 Pct Recovery = 109% Analysis Date = 01/03/18 Pct Recovery = 109% Analysis Date = 01/03/18 Pct Recovery = 109% Analysis Date = 12/24/17 Pct Recovery = 109% Analysis Date = 12/24/17 Pct Recovery = 109% Analysis Date = 12/15/17 Pct Recovery = 108% Analysis Date = 12/15/17 Pct Recovery = 108% Analysis Date = 12/06/17 Pct Recovery = 108% Analysis Date = 12/06/17 Pct Recovery = 108% Analysis Date = 11/26/17 Pct Recovery = 108% Analysis Date = 11/26/17 Pct Recovery = 108% Analysis Date = 11/17/17 Pct Recovery = 108% Analysis Date = 11/17/17 Pct Recovery = 108% Analysis Date = 11/07/17 Pct Recovery = 107% Analysis Date = 11/07/17 Pct Recovery = 107% Analysis Date = 10/29/17 Pct Recovery = 107% Analysis Date = 10/29/17 Pct Recovery = 107% Analysis Date = 10/20/17 Pct Recovery = 107% Analysis Date = 10/20/17 Pct Recovery = 107% Analysis Date = 10/10/17 Pct Recovery = 107% Analysis Date = 10/10/17 Pct Recovery = 107% Analysis Date = 10/01/17 Pct Recovery = 106% Analysis Date = 10/01/17 Pct Recovery = 106% Analysis Date = 09/21/17 Pct Recovery = 106% Analysis Date = 09/21/17 Pct Recovery = 106% Analysis Date = 09/12/17 Pct Recovery = 106% Analysis Date = 09/12/17 Pct Recovery = 106% Analysis Date = 09/03/17 Pct Recovery = 106% Analysis Date = 09/03/17 Pct Recovery = 106% Analysis Date = 08/24/17 Pct Recovery = 106% Analysis Date = 08/24/17 Pct Recovery = 106% Analysis Date = 08/15/17 Pct Recovery = 105% Analysis Date = 08/15/17 Pct Recovery = 105% Analysis Date = 08/05/17 Pct Recovery = 105% Analysis Date = 08/05/17 Pct Recovery = 105% Analysis Date = 07/27/17 Pct Recovery = 105% Analysis Date = 07/27/17 Pct Recovery = 105% Analysis Date = 07/18/17 Pct Recovery = 105% Analysis Date = 07/18/17 Pct Recovery = 105% Analysis Date = 07/08/17 Pct Recovery = 104% Analysis Date = 07/08/17 Pct Recovery = 104% Analysis Date = 06/29/17 Pct Recovery = 104% Analysis Date = 06/29/17 Pct Recovery = 104% Analysis Date = 06/19/17 Pct Recovery = 104% Analysis Date = 06/19/17 Pct Recovery = 104% Analysis Date = 06/10/17 Pct Recovery = 104% Analysis Date = 06/10/17 Pct Recovery = 104% Analysis Date = 06/01/17 Pct Recovery = 103% Analysis Date = 06/01/17 Pct Recovery = 103% Analysis Date = 05/22/17 Pct Recovery = 103% Analysis Date = 05/22/17 Pct Recovery = 103% Analysis Date = 05/13/17 Pct Recovery = 103% Analysis Date = 05/13/17 Pct Recovery = 103% Analysis Date = 05/03/17 Pct Recovery = 103% Analysis Date = 05/03/17 Pct Recovery = 103% Analysis Date = 04/24/17 Pct Recovery = 102% Analysis Date = 04/24/17 Pct Recovery = 102% Analysis Date = 04/15/17 Pct Recovery = 102% Analysis Date = 04/15/17 Pct Recovery = 102% Analysis Date = 04/05/17 Pct Recovery = 102% Analysis Date = 04/05/17 Pct Recovery = 102% Analysis Date = 03/27/17 Pct Recovery = 102% Analysis Date = 03/27/17 Pct Recovery = 102% Analysis Date = 03/17/17 Pct Recovery = 102% Analysis Date = 03/17/17 Pct Recovery = 102% Analysis Date = 03/08/17 Pct Recovery = 101% Analysis Date = 03/08/17 Pct Recovery = 101% Analysis Date = 02/27/17 Pct Recovery = 101% Analysis Date = 02/27/17 Pct Recovery = 101% Analysis Date = 02/17/17 Pct Recovery = 101% Analysis Date = 02/17/17 Pct Recovery = 101% Analysis Date = 02/08/17 Pct Recovery = 101% Analysis Date = 02/08/17 Pct Recovery = 101% Analysis Date = 01/29/17 Pct Recovery = 100% Analysis Date = 01/29/17 Pct Recovery = 100% Analysis Date = 01/20/17 Pct Recovery = 100% Analysis Date = 01/20/17 Pct Recovery = 100% Analysis Date = 01/11/17 Pct Recovery = 100% Analysis Date = 01/11/17 Pct Recovery = 100% Analysis Date = 01/01/17 Pct Recovery = 100% Analysis Date = 01/01/17 Pct Recovery = 100% Analysis Date = 12/23/16 Pct Recovery = 100% Analysis Date = 12/23/16 Pct Recovery = 100% Analysis Date = 12/13/16 Pct Recovery = 99% Analysis Date = 12/13/16 Pct Recovery = 99% Analysis Date = 12/04/16 Pct Recovery = 99% Analysis Date = 12/04/16 Pct Recovery = 99% Analysis Date = 11/25/16 Pct Recovery = 99% Analysis Date = 11/25/16 Pct Recovery = 99% Analysis Date = 11/15/16 Pct Recovery = 99% Analysis Date = 11/15/16 Pct Recovery = 99% Analysis Date = 11/06/16 Pct Recovery = 98% Analysis Date = 11/06/16 Pct Recovery = 98% Analysis Date = 10/27/16 Pct Recovery = 98% Analysis Date = 10/27/16 Pct Recovery = 98% Analysis Date = 10/18/16 Pct Recovery = 98% Analysis Date = 10/18/16 Pct Recovery = 98% Analysis Date = 10/09/16 Pct Recovery = 98% Analysis Date = 10/09/16 Pct Recovery = 98% Analysis Date = 09/29/16 Pct Recovery = 98% Analysis Date = 09/29/16 Pct Recovery = 98% Analysis Date = 09/20/16 Pct Recovery = 97% Analysis Date = 09/20/16 Pct Recovery = 97% Analysis Date = 09/10/16 Pct Recovery = 97% Analysis Date = 09/10/16 Pct Recovery = 97% Analysis Date = 09/01/16 Pct Recovery = 97% Analysis Date = 09/01/16 Pct Recovery = 97% Analysis Date = 08/23/16 Pct Recovery = 97% Analysis Date = 08/23/16 Pct Recovery = 97% Analysis Date = 08/13/16 Pct Recovery = 97% Analysis Date = 08/13/16 Pct Recovery = 97% Analysis Date = 08/04/16 Pct Recovery = 96% Analysis Date = 08/04/16 Pct Recovery = 96% Analysis Date = 07/25/16 Pct Recovery = 96% Analysis Date = 07/25/16 Pct Recovery = 96% Analysis Date = 07/16/16 Pct Recovery = 96% Analysis Date = 07/16/16 Pct Recovery = 96% Analysis Date = 07/07/16 Pct Recovery = 96% Analysis Date = 07/07/16 Pct Recovery = 96% Analysis Date = 06/27/16 Pct Recovery = 96% Analysis Date = 06/27/16 Pct Recovery = 96% Analysis Date = 06/18/16 Pct Recovery = 96% Analysis Date = 06/18/16 Pct Recovery = 96% Analysis Date = 06/08/16 Pct Recovery = 96% Analysis Date = 06/08/16 Pct Recovery = 96% Analysis Date = 05/30/16 Pct Recovery = 95% Analysis Date = 05/30/16 Pct Recovery = 95% Analysis Date = 05/21/16 Pct Recovery = 95% Analysis Date = 05/21/16 Pct Recovery = 95% Analysis Date = 05/11/16 Pct Recovery = 95% Analysis Date = 05/11/16 Pct Recovery = 95% Analysis Date = 05/02/16 Pct Recovery = 95% Analysis Date = 05/02/16 Pct Recovery = 95% Analysis Date = 04/22/16 Pct Recovery = 95% Analysis Date = 04/22/16 Pct Recovery = 95% Analysis Date = 04/13/16 Pct Recovery = 95% Analysis Date = 04/13/16 Pct Recovery = 95% Analysis Date = 04/04/16 Pct Recovery = 95% Analysis Date = 04/04/16 Pct Recovery = 95% Analysis Date = 03/25/16 Pct Recovery = 94% Analysis Date = 03/25/16 Pct Recovery = 94% Analysis Date = 03/16/16 Pct Recovery = 94% Analysis Date = 03/16/16 Pct Recovery = 94% Analysis Date = 03/06/16 Pct Recovery = 94% Analysis Date = 03/06/16 Pct Recovery = 94% Analysis Date = 02/26/16 Pct Recovery = 94% Analysis Date = 02/26/16 Pct Recovery = 94% Analysis Date = 02/17/16 Pct Recovery = 94% Analysis Date = 02/17/16 Pct Recovery = 94% Analysis Date = 02/07/16 Pct Recovery = 94% Analysis Date = 02/07/16 Pct Recovery = 94% Analysis Date = 01/29/16 Pct Recovery = 94% Analysis Date = 01/29/16 Pct Recovery = 94% Analysis Date = 01/19/16 Pct Recovery = 94% Analysis Date = 01/19/16 Pct Recovery = 94% Analysis Date = 01/10/16 Pct Recovery = 93% Analysis Date = 01/10/16 Pct Recovery = 93% Analysis Date = 01/01/16 Pct Recovery = 93% Analysis Date = 01/01/16 Pct Recovery = 93% Analysis Date = 12/22/15 Pct Recovery = 93% Analysis Date = 12/22/15 Pct Recovery = 93% Analysis Date = 12/13/15 Pct Recovery = 93% Analysis Date = 12/13/15 Pct Recovery = 93% Analysis Date = 12/03/15 Pct Recovery = 93% Analysis Date = 12/03/15 Pct Recovery = 93% Analysis Date = 11/24/15 Pct Recovery = 93% Analysis Date = 11/24/15 Pct Recovery = 93% Analysis Date = 11/15/15 Pct Recovery = 93% Analysis Date = 11/15/15 Pct Recovery = 93% Analysis Date = 11/05/15 Pct Recovery = 92% Analysis Date = 11/05/15 Pct Recovery = 92% Analysis Date = 10/27/15 Pct Recovery = 92% Analysis Date = 10/27/15 Pct Recovery = 92% Analysis Date = 10/17/15 Pct Recovery = 92% Analysis Date = 10/17/15 Pct Recovery = 92% Analysis Date = 10/08/15 Pct Recovery = 92% Analysis Date = 10/08/15 Pct Recovery = 92% Analysis Date = 09/29/15 Pct Recovery = 92% Analysis Date = 09/29/15 Pct Recovery = 92% Analysis Date = 09/19/15 Pct Recovery = 92% Analysis Date = 09/19/15 Pct Recovery = 92% Analysis Date = 09/10/15 Pct Recovery = 92% Analysis Date = 09/10/15 Pct Recovery = 92% Analysis Date = 08/31/15 Pct Recovery = 91% Analysis Date = 08/31/15 Pct Recovery = 91% Analysis Date = 08/22/15 Pct Recovery = 91% Analysis Date = 08/22/15 Pct Recovery = 91% Analysis Date = 08/13/15 Pct Recovery = 91% Analysis Date = 08/13/15 Pct Recovery = 91% Analysis Date = 08/03/15 Pct Recovery = 91% Analysis Date = 08/03/15 Pct Recovery = 91% Analysis Date = 07/25/15 Pct Recovery = 91% Analysis Date = 07/25/15 Pct Recovery = 91% Analysis Date = 07/15/15 Pct Recovery = 91% Analysis Date = 07/15/15 Pct Recovery = 91% Analysis Date = 07/06/15 Pct Recovery = 91% Analysis Date = 07/06/15 Pct Recovery = 91% Analysis Date = 06/27/15 Pct Recovery = 91% Analysis Date = 06/27/15 Pct Recovery = 91% Analysis Date = 06/17/15 Pct Recovery = 91% Analysis Date = 06/17/15 Pct Recovery = 91% Analysis Date = 06/08/15 Pct Recovery = 90% Analysis Date = 06/08/15 Pct Recovery = 90% Analysis Date = 05/29/15 Pct Recovery = 90% Analysis Date = 05/29/15 Pct Recovery = 90% Analysis Date = 05/20/15 Pct Recovery = 90% Analysis Date = 05/20/15 Pct Recovery = 90% Analysis Date = 05/11/15 Pct Recovery = 90% Analysis Date = 05/11/15 Pct Recovery = 90% Analysis Date = 05/01/15 Pct Recovery = 90% Analysis Date = 05/01/15 Pct Recovery = 90% Analysis Date = 04/22/15 Pct Recovery = 90% Analysis Date = 04/22/15 Pct Recovery = 90% Analysis Date = 04/12/15 Pct Recovery = 90% Analysis Date = 04/12/15 Pct Recovery = 90% Analysis Date = 04/03/15 Pct Recovery = 90% Analysis Date = 04/03/15 Pct Recovery = 90% Analysis Date = 03/25/15 Pct Recovery = 90% Analysis Date = 03/25/15 Pct Recovery = 90% Analysis Date = 03/15/15 Pct Recovery = 90% Analysis Date = 03/15/15 Pct Recovery = 90% Analysis Date = 03/06/15 Pct Recovery = 90% Analysis Date = 03/06/15 Pct Recovery = 90% Analysis Date = 02/24/15 Pct Recovery = 90% Analysis Date = 02/24/15 Pct Recovery = 90% Analysis Date = 02/15/15 Pct Recovery = 90% Analysis Date = 02/15/15 Pct Recovery = 90% Analysis Date = 02/06/15 Pct Recovery = 90% Analysis Date = 02/06/15 Pct Recovery = 90% Analysis Date = 01/27/15 Pct Recovery = 90% Analysis Date = 01/27/15 Pct Recovery = 90% Analysis Date = 01/18/15 Pct Recovery = 90% Analysis Date = 01/18/15 Pct Recovery = 90% Analysis Date = 01/08/15 Pct Recovery = 90% Analysis Date = 01/08/15 Pct Recovery = 90% Analysis Date = 12/30/14 Pct Recovery = 90% Analysis Date = 12/30/14 Pct Recovery = 90% Analysis Date = 12/21/14 Pct Recovery = 90% Analysis Date = 12/21/14 Pct Recovery = 90% Analysis Date = 12/11/14 Pct Recovery = 90% Analysis Date = 12/11/14 Pct Recovery = 90% Analysis Date = 12/02/14 Pct Recovery = 90% Analysis Date = 12/02/14 Pct Recovery = 90% Analysis Date = 11/22/14 Pct Recovery = 90% Analysis Date = 11/22/14 Pct Recovery = 90% Analysis Date = 11/13/14 Pct Recovery = 90% Analysis Date = 11/13/14 Pct Recovery = 90% Analysis Date = 11/04/14 Pct Recovery = 90% Analysis Date = 11/04/14 Pct Recovery = 90% Analysis Date = 10/25/14 Pct Recovery = 90% Analysis Date = 10/25/14 Pct Recovery = 90% Analysis Date = 10/16/14 Pct Recovery = 90% Analysis Date = 10/16/14 Pct Recovery = 90% Analysis Date = 10/06/14 Pct Recovery = 90% Analysis Date = 10/06/14 Pct Recovery = 90% Analysis Date = 09/27/14 Pct Recovery = 90% Analysis Date = 09/27/14 Pct Recovery = 90% Analysis Date = 09/18/14 Pct Recovery = 90% Analysis Date = 09/18/14 Pct Recovery = 90% Analysis Date = 09/08/14 Pct Recovery = 90% Analysis Date = 09/08/14 Pct Recovery = 90% Analysis Date = 08/30/14 Pct Recovery = 90% Analysis Date = 08/30/14 Pct Recovery = 90% Analysis Date = 08/20/14 Pct Recovery = 90% Analysis Date = 08/20/14 Pct Recovery = 90% Analysis Date = 08/11/14 Pct Recovery = 90% Analysis Date = 08/11/14 Pct Recovery = 90% Analysis Date = 08/02/14 Pct Recovery = 90% Analysis Date = 08/02/14 Pct Recovery = 90% Analysis Date = 07/23/14 Pct Recovery = 90% Analysis Date = 07/23/14 Pct Recovery = 90% Analysis Date = 07/14/14 Pct Recovery = 90% Analysis Date = 07/14/14 Pct Recovery = 90% Analysis Date = 07/04/14 Pct Recovery = 90% Analysis Date = 07/04/14 Pct Recovery = 90% Analysis Date = 06/25/14 Pct Recovery = 90% Analysis Date = 06/25/14 Pct Recovery = 90% Analysis Date = 06/16/14 Pct Recovery = 90% Analysis Date = 06/16/14 Pct Recovery = 90% Analysis Date = 06/06/14 Pct Recovery = 90% Analysis Date = 06/06/14 Pct Recovery = 90% Analysis Date = 05/28/14 Pct Recovery = 90% Analysis Date = 05/28/14 Pct Recovery = 90% Analysis Date = 05/18/14 Pct Recovery = 90% Analysis Date = 05/18/14 Pct Recovery = 90% Analysis Date = 05/09/14 Pct Recovery = 91% Analysis Date = 05/09/14 Pct Recovery = 91% Analysis Date = 04/30/14 Pct Recovery = 91% Analysis Date = 04/30/14 Pct Recovery = 91% Analysis Date = 04/20/14 Pct Recovery = 91% Analysis Date = 04/20/14 Pct Recovery = 91% Analysis Date = 04/11/14 Pct Recovery = 91% Analysis Date = 04/11/14 Pct Recovery = 91% Analysis Date = 04/01/14 Pct Recovery = 91% Analysis Date = 04/01/14 Pct Recovery = 91% Analysis Date = 03/23/14 Pct Recovery = 91% Analysis Date = 03/23/14 Pct Recovery = 91% Analysis Date = 03/14/14 Pct Recovery = 91% Analysis Date = 03/14/14 Pct Recovery = 91% Analysis Date = 03/04/14 Pct Recovery = 91% Analysis Date = 03/04/14 Pct Recovery = 91% Analysis Date = 02/23/14 Pct Recovery = 91% Analysis Date = 02/23/14 Pct Recovery = 91% Analysis Date = 02/13/14 Pct Recovery = 91% Analysis Date = 02/13/14 Pct Recovery = 91% Analysis Date = 02/04/14 Pct Recovery = 92% Analysis Date = 02/04/14 Pct Recovery = 92% Analysis Date = 01/26/14 Pct Recovery = 92% Analysis Date = 01/26/14 Pct Recovery = 92% Analysis Date = 01/16/14 Pct Recovery = 92% Analysis Date = 01/16/14 Pct Recovery = 92% Analysis Date = 01/07/14 Pct Recovery = 92% Analysis Date = 01/07/14 Pct Recovery = 92% Analysis Date = 12/28/13 Pct Recovery = 92% Analysis Date = 12/28/13 Pct Recovery = 92% Analysis Date = 12/19/13 Pct Recovery = 92% Analysis Date = 12/19/13 Pct Recovery = 92% Analysis Date = 12/10/13 Pct Recovery = 92% Analysis Date = 12/10/13 Pct Recovery = 92% Analysis Date = 11/30/13 Pct Recovery = 92% Analysis Date = 11/30/13 Pct Recovery = 92% Analysis Date = 11/21/13 Pct Recovery = 92% Analysis Date = 11/21/13 Pct Recovery = 92% Analysis Date = 11/11/13 Pct Recovery = 92% Analysis Date = 11/11/13 Pct Recovery = 92% Analysis Date = 11/02/13 Pct Recovery = 92% Analysis Date = 11/02/13 Pct Recovery = 92% Analysis Date = 10/24/13 Pct Recovery = 92% Analysis Date = 10/24/13 Pct Recovery = 92% Analysis Date = 10/14/13 Pct Recovery = 91% Analysis Date = 10/14/13 Pct Recovery = 91% Analysis Date = 10/05/13 Pct Recovery = 91% Analysis Date = 10/05/13 Pct Recovery = 91% Analysis Date = 09/25/13 Pct Recovery = 91% Analysis Date = 09/25/13 Pct Recovery = 91% Analysis Date = 09/16/13 Pct Recovery = 91% Analysis Date = 09/16/13 Pct Recovery = 91% Analysis Date = 09/07/13 Pct Recovery = 91% Analysis Date = 09/07/13 Pct Recovery = 91% Analysis Date = 08/28/13 Pct Recovery = 91% Analysis Date = 08/28/13 Pct Recovery = 91% Analysis Date = 08/19/13 Pct Recovery = 91% Analysis Date = 08/19/13 Pct Recovery = 91% Analysis Date = 08/09/13 Pct Recovery = 91% Analysis Date = 08/09/13 Pct Recovery = 91% Analysis Date = 07/31/13 Pct Recovery = 91% Analysis Date = 07/31/13 Pct Recovery = 91% Analysis Date = 07/22/13 Pct Recovery = 91% Analysis Date = 07/22/13 Pct Recovery = 91% Analysis Date = 07/12/13 Pct Recovery = 91% Analysis Date = 07/12/13 Pct Recovery = 91% Analysis Date = 07/03/13 Pct Recovery = 91% Analysis Date = 07/03/13 Pct Recovery = 91% Analysis Date = 06/23/13 Pct Recovery = 91% Analysis Date = 06/23/13 Pct Recovery = 91% Analysis Date = 06/14/13 Pct Recovery = 91% Analysis Date = 06/14/13 Pct Recovery = 91% Analysis Date = 06/05/13 Pct Recovery = 91% Analysis Date = 06/05/13 Pct Recovery = 91% Analysis Date = 05/26/13 Pct Recovery = 91% Analysis Date = 05/26/13 Pct Recovery = 91% Analysis Date = 05/17/13 Pct Recovery = 91% Analysis Date = 05/17/13 Pct Recovery = 91% Analysis Date = 05/07/13 Pct Recovery = 91% Analysis Date = 05/07/13 Pct Recovery = 91% Analysis Date = 04/28/13 Pct Recovery = 91% Analysis Date = 04/28/13 Pct Recovery = 91% Analysis Date = 04/19/13 Pct Recovery = 91% Analysis Date = 04/19/13 Pct Recovery = 91% Analysis Date = 04/09/13 Pct Recovery = 91% Analysis Date = 04/09/13 Pct Recovery = 91% Analysis Date = 03/31/13 Pct Recovery = 91% Analysis Date = 03/31/13 Pct Recovery = 91% Analysis Date = 03/21/13 Pct Recovery = 91% Analysis Date = 03/21/13 Pct Recovery = 91% Analysis Date = 03/12/13 Pct Recovery = 91% Analysis Date = 03/12/13 Pct Recovery = 91% Analysis Date = 03/03/13 Pct Recovery = 91% Analysis Date = 03/03/13 Pct Recovery = 91% Analysis Date = 02/21/13 Pct Recovery = 90% Analysis Date = 02/21/13 Pct Recovery = 90% Analysis Date = 02/12/13 Pct Recovery = 90% Analysis Date = 02/12/13 Pct Recovery = 90% Analysis Date = 02/02/13 Pct Recovery = 90% Analysis Date = 02/02/13 Pct Recovery = 90% Analysis Date = 01/24/13 Pct Recovery = 90% Analysis Date = 01/24/13 Pct Recovery = 90% Analysis Date = 01/15/13 Pct Recovery = 90% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
SIMAZINE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 78 94% 17% 92% 14%
Total 78 94% 17% 92% 14%

Sample Statistics
SIMAZINE

Characteristic N % % Basis
Plotted 78 100% Spiked
Estimated Values 5 6% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 78 .  
False Negatives 0 0% 0 out of 78
Not Spiked 40 .  
False Positives 0 0% 0 out of 40

OBSP Determination:
TEBUCONAZOLE
METHOD: 2033 , TESTIDCODE: 62852GCM14

Laboratory ID = 20130250061 Lab Value = 0.158 Expected Conc. = 0.298 Report level label = 0.02 Pct Recovery = 53% Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl SpecificMix = 05BB029 Laboratory ID = 20140100085 Lab Value = 0.130 Expected Conc. = 0.202 Report level label = 0.02 Pct Recovery = 64% Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl SpecificMix = 042413 Laboratory ID = 20140230082 Lab Value = 0.081 Expected Conc. = 0.1505 Report level label = 0.02 Pct Recovery = 54% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl SpecificMix = 012513 Laboratory ID = 20132420001 Lab Value = 0.074 Expected Conc. = 0.1505 Report level label = 0.02 Pct Recovery = 49% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl SpecificMix = 012513 Laboratory ID = 20130940097 Lab Value = 0.084 Expected Conc. = 0.15 Report level label = 0.02 Pct Recovery = 56% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = 052412 Laboratory ID = 20130100066 Lab Value = 0.152 Expected Conc. = 0.15 Report level label = 0.02 Pct Recovery = 101% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl SpecificMix = 052412 Laboratory ID = 20172510330 Lab Value = 0.070 Expected Conc. = 0.133 Report level label = 0.02 Pct Recovery = 52% Analysis Date = 12/29/17 SpikeMix = ChemService 6537100: 100 µl & Abs 071817Pest: 100 µl SpecificMix = 071817Pest Laboratory ID = 20162860079 Lab Value = 0.068 Expected Conc. = 0.125 Report level label = 0.02 Pct Recovery = 54% Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl SpecificMix = 060916 Laboratory ID = 20163150006 Lab Value = 0.076 Expected Conc. = 0.125 Report level label = 0.02 Pct Recovery = 61% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl SpecificMix = 060916 Laboratory ID = 20152750006 Lab Value = 0.105 Expected Conc. = 0.12 Report level label = 0.02 Pct Recovery = 88% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl SpecificMix = EN150514012 Laboratory ID = 20152460215 Lab Value = 0.080 Expected Conc. = 0.12 Report level label = 0.02 Pct Recovery = 67% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl SpecificMix = EN150514012 Laboratory ID = 20171380001 Lab Value = 0.054 Expected Conc. = 0.1016 Report level label = 0.02 Pct Recovery = 53% Analysis Date = 06/07/17 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 041816 Laboratory ID = 20170740063 Lab Value = 0.084 Expected Conc. = 0.1016 Report level label = 0.02 Pct Recovery = 83% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl SpecificMix = 041816 Laboratory ID = 20161740258 Lab Value = 0.054 Expected Conc. = 0.1016 Report level label = 0.02 Pct Recovery = 53% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 041816 Laboratory ID = 20132690010 Lab Value = 0.073 Expected Conc. = 0.101 Report level label = 0.02 Pct Recovery = 72% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl SpecificMix = 042413 Laboratory ID = 20132560001 Lab Value = 0.060 Expected Conc. = 0.101 Report level label = 0.02 Pct Recovery = 60% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl SpecificMix = 042413 Laboratory ID = 20171660002 Lab Value = 0.057 Expected Conc. = 0.1 Report level label = 0.02 Pct Recovery = 57% Analysis Date = 08/23/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = 060916 Laboratory ID = 20170190026 Lab Value = 0.061 Expected Conc. = 0.1 Report level label = 0.02 Pct Recovery = 61% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = 060916 Laboratory ID = 20132140002 Lab Value = 0.054 Expected Conc. = 0.0995 Report level label = 0.02 Pct Recovery = 54% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl SpecificMix = 04CC101 Laboratory ID = 20150430092 Lab Value = 0.064 Expected Conc. = 0.0798 Report level label = 0.02 Pct Recovery = 81% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl SpecificMix = 042814 Laboratory ID = 20143240095 Lab Value = 0.043 Expected Conc. = 0.0798 Report level label = 0.02 Pct Recovery = 54% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl SpecificMix = 042814 Laboratory ID = 20142960086 Lab Value = 0.047 Expected Conc. = 0.0798 Report level label = 0.02 Pct Recovery = 59% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 042814 Laboratory ID = 20142530087 Lab Value = 0.038 Expected Conc. = 0.0798 Report level label = 0.02 Pct Recovery = 47% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl SpecificMix = 042814 Laboratory ID = 20150720069 Lab Value = 0.066 Expected Conc. = 0.0786 Report level label = 0.02 Pct Recovery = 83% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 0227-14-08 Laboratory ID = 20141770149 Lab Value = 0.046 Expected Conc. = 0.0786 Report level label = 0.02 Pct Recovery = 58% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl SpecificMix = 0227-14-08 Laboratory ID = 20141570088 Lab Value = 0.040 Expected Conc. = 0.0786 Report level label = 0.02 Pct Recovery = 51% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl SpecificMix = 0227-14-08 Laboratory ID = 20181430122 Lab Value = 0.045 Expected Conc. = 0.0665 Report level label = 0.02 Pct Recovery = 68% Analysis Date = 06/20/18 SpikeMix = Abs 071817Pest: 50 µl & Spex Organics EN170808006: 50 µl SpecificMix = 071817Pest Laboratory ID = 20173480003 Lab Value = 0.034 Expected Conc. = 0.065 Report level label = 0.02 Pct Recovery = 52% Analysis Date = 04/05/18 SpikeMix = Abs 071717Pest: 50 µl & ChemService 6567600: 50 µl SpecificMix = 6567600 Laboratory ID = 20172560101 Lab Value = 0.040 Expected Conc. = 0.065 Report level label = 0.02 Pct Recovery = 61% Analysis Date = 12/22/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6567600: 50 µl SpecificMix = 6567600 Laboratory ID = 20152330039 Lab Value = 0.046 Expected Conc. = 0.0604 Report level label = 0.02 Pct Recovery = 75% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl SpecificMix = 041415 Laboratory ID = 20151900132 Lab Value = 0.065 Expected Conc. = 0.0604 Report level label = 0.02 Pct Recovery = 108% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl SpecificMix = 041415 Laboratory ID = 20151270112 Lab Value = 0.047 Expected Conc. = 0.0604 Report level label = 0.02 Pct Recovery = 78% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl SpecificMix = 041415 Laboratory ID = 20140860102 Lab Value = 0.027 Expected Conc. = 0.0602 Report level label = 0.02 Pct Recovery = 44% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 012513 Laboratory ID = 20131920149 Lab Value = 0.033 Expected Conc. = 0.0602 Report level label = 0.02 Pct Recovery = 54% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl SpecificMix = 012513 Laboratory ID = 20160630046 Lab Value = 0.038 Expected Conc. = 0.06 Report level label = 0.02 Pct Recovery = 64% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = EN150514012 Laboratory ID = 20153440001 Lab Value = 0.034 Expected Conc. = 0.06 Report level label = 0.02 Pct Recovery = 56% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = EN150514012 Laboratory ID = 20133400002 Lab Value = 0.031 Expected Conc. = 0.06 Report level label = 0.02 Pct Recovery = 51% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = 052412 Laboratory ID = 20132910008 Lab Value = 0.034 Expected Conc. = 0.06 Report level label = 0.02 Pct Recovery = 57% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = 052412 Laboratory ID = 20130650005 Lab Value = 0.031 Expected Conc. = 0.06 Report level label = 0.02 Pct Recovery = 52% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl SpecificMix = 052412 Laboratory ID = 20131230084 Lab Value = 0.044 Expected Conc. = 0.0596 Report level label = 0.02 Pct Recovery = 74% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl SpecificMix = 05BB029 Laboratory ID = 20130510051 Lab Value = 0.038 Expected Conc. = 0.0596 Report level label = 0.02 Pct Recovery = 64% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl SpecificMix = 05BB029 Laboratory ID = 20171940002 Lab Value = 0.036 Expected Conc. = 0.0508 Report level label = 0.02 Pct Recovery = 72% Analysis Date = 11/10/17 SpikeMix = ChemService 5054800: 40 µl & NSI 041816: 40 µl SpecificMix = 041816 Laboratory ID = 20162020124 Lab Value = 0.028 Expected Conc. = 0.0508 Report level label = 0.02 Pct Recovery = 55% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl SpecificMix = 041816 Laboratory ID = 20161600087 Lab Value = 0.033 Expected Conc. = 0.0508 Report level label = 0.02 Pct Recovery = 66% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 041816 Laboratory ID = 20161340228 Lab Value = 0.035 Expected Conc. = 0.0508 Report level label = 0.02 Pct Recovery = 69% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl SpecificMix = 041816 Laboratory ID = 20161190075 Lab Value = 0.035 Expected Conc. = 0.0508 Report level label = 0.02 Pct Recovery = 68% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 041816 Laboratory ID = 20171160110 Lab Value = 0.039 Expected Conc. = 0.05 Report level label = 0.02 Pct Recovery = 78% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = 060916 Laboratory ID = 20162520001 Lab Value = 0.036 Expected Conc. = 0.05 Report level label = 0.02 Pct Recovery = 71% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl SpecificMix = 060916 Laboratory ID = 20163560019 Lab Value = 0.041 Expected Conc. = 0.05 Report level label = 0.02 Pct Recovery = 82% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl SpecificMix = 060916 Laboratory ID = 20162380004 Lab Value = 0.026 Expected Conc. = 0.05 Report level label = 0.02 Pct Recovery = 52% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = 060916 Laboratory ID = 20133580036 Lab Value = 0.019 Expected Conc. = 0.0404 Report level label = 0.02 Pct Recovery = 48% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 042413 Laboratory ID = 20133190012 Lab Value = 0.027 Expected Conc. = 0.0404 Report level label = 0.02 Pct Recovery = 66% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 042413 Laboratory ID = 20131650073 Lab Value = 0.036 Expected Conc. = 0.0404 Report level label = 0.02 Pct Recovery = 90% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl SpecificMix = 042413 Laboratory ID = 20180730064 Lab Value = 0.027 Expected Conc. = 0.0399 Report level label = 0.02 Pct Recovery = 67% Analysis Date = 05/16/18 SpikeMix = Abs 071717Pest: 30 µl & Abs 071817Pest: 30 µl SpecificMix = 071817Pest Laboratory ID = 20180050004 Lab Value = 0.020 Expected Conc. = 0.0399 Report level label = 0.02 Pct Recovery = 50% Analysis Date = 04/05/18 SpikeMix = Abs 071817Pest: 30 µl & ChemService 6472100: 30 µl SpecificMix = 071817Pest Laboratory ID = 20172780018 Lab Value = 0.027 Expected Conc. = 0.0399 Report level label = 0.02 Pct Recovery = 68% Analysis Date = 02/08/18 SpikeMix = ChemService 6537100: 30 µl & Abs 071817Pest: 30 µl SpecificMix = 071817Pest Laboratory ID = 20143370094 Lab Value = 0.021 Expected Conc. = 0.0399 Report level label = 0.02 Pct Recovery = 54% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl SpecificMix = 042814 Laboratory ID = 20142820151 Lab Value = 0.027 Expected Conc. = 0.0399 Report level label = 0.02 Pct Recovery = 69% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl SpecificMix = 042814 Laboratory ID = 20142470041 Lab Value = 0.024 Expected Conc. = 0.0399 Report level label = 0.02 Pct Recovery = 60% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl SpecificMix = 042814 Laboratory ID = 20142200164 Lab Value = 0.026 Expected Conc. = 0.0399 Report level label = 0.02 Pct Recovery = 66% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 042814 Laboratory ID = 20140730138 Lab Value = 0.027 Expected Conc. = 0.0398 Report level label = 0.02 Pct Recovery = 68% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 04CC101 Laboratory ID = 20140510043 Lab Value = 0.038 Expected Conc. = 0.0398 Report level label = 0.02 Pct Recovery = 96% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 04CC101 Laboratory ID = 20133310030 Lab Value = 0.028 Expected Conc. = 0.0398 Report level label = 0.02 Pct Recovery = 70% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl SpecificMix = 04CC101 Laboratory ID = 20132280016 Lab Value = 0.031 Expected Conc. = 0.0398 Report level label = 0.02 Pct Recovery = 78% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl SpecificMix = 04CC101 Laboratory ID = 20131510026 Lab Value = 0.034 Expected Conc. = 0.0398 Report level label = 0.02 Pct Recovery = 85% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl SpecificMix = 04CC101 Laboratory ID = 20141840097 Lab Value = 0.023 Expected Conc. = 0.0393 Report level label = 0.02 Pct Recovery = 58% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20141490205 Lab Value = 0.019 Expected Conc. = 0.0393 Report level label = 0.02 Pct Recovery = 48% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20141420140 Lab Value = 0.021 Expected Conc. = 0.0393 Report level label = 0.02 Pct Recovery = 52% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20141360094 Lab Value = 0.021 Expected Conc. = 0.0393 Report level label = 0.02 Pct Recovery = 53% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20161050143 Lab Value = 0.020 Expected Conc. = 0.0302 Report level label = 0.02 Pct Recovery = 67% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 041415 Laboratory ID = 20160560044 Lab Value = 0.019 Expected Conc. = 0.0302 Report level label = 0.02 Pct Recovery = 62% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl SpecificMix = 041415 Laboratory ID = 20160210080 Lab Value = 0.015 Expected Conc. = 0.0302 Report level label = 0.02 Pct Recovery = 48% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 041415 Laboratory ID = 20152950078 Lab Value = 0.013 Expected Conc. = 0.0302 Report level label = 0.02 Pct Recovery = 44% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 041415 Laboratory ID = 20152040177 Lab Value = 0.032 Expected Conc. = 0.0302 Report level label = 0.02 Pct Recovery = 107% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl SpecificMix = 041415 Laboratory ID = 20151210037 Lab Value = 0.024 Expected Conc. = 0.0302 Report level label = 0.02 Pct Recovery = 79% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 041415 Laboratory ID = 20160070059 Lab Value = 0.023 Expected Conc. = 0.03 Report level label = 0.02 Pct Recovery = 78% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = EN150514012 Laboratory ID = 20153160001 Lab Value = 0.019 Expected Conc. = 0.03 Report level label = 0.02 Pct Recovery = 64% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = EN150514012 Laboratory ID = 20151760208 Lab Value = 0.031 Expected Conc. = 0.03 Report level label = 0.02 Pct Recovery = 104% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl SpecificMix = EN150514012 Laboratory ID = 20151480170 Lab Value = 0.021 Expected Conc. = 0.03 Report level label = 0.02 Pct Recovery = 69% Analysis Date = 06/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150514012 Analysis Date = 06/20/18 Pct Recovery = 60% Analysis Date = 06/10/18 Pct Recovery = 60% Analysis Date = 06/10/18 Pct Recovery = 60% Analysis Date = 05/31/18 Pct Recovery = 60% Analysis Date = 05/31/18 Pct Recovery = 60% Analysis Date = 05/21/18 Pct Recovery = 60% Analysis Date = 05/21/18 Pct Recovery = 60% Analysis Date = 05/11/18 Pct Recovery = 60% Analysis Date = 05/11/18 Pct Recovery = 60% Analysis Date = 05/01/18 Pct Recovery = 60% Analysis Date = 05/01/18 Pct Recovery = 60% Analysis Date = 04/21/18 Pct Recovery = 60% Analysis Date = 04/21/18 Pct Recovery = 60% Analysis Date = 04/11/18 Pct Recovery = 60% Analysis Date = 04/11/18 Pct Recovery = 60% Analysis Date = 04/01/18 Pct Recovery = 60% Analysis Date = 04/01/18 Pct Recovery = 60% Analysis Date = 03/22/18 Pct Recovery = 60% Analysis Date = 03/22/18 Pct Recovery = 60% Analysis Date = 03/13/18 Pct Recovery = 61% Analysis Date = 03/13/18 Pct Recovery = 61% Analysis Date = 03/03/18 Pct Recovery = 61% Analysis Date = 03/03/18 Pct Recovery = 61% Analysis Date = 02/21/18 Pct Recovery = 61% Analysis Date = 02/21/18 Pct Recovery = 61% Analysis Date = 02/11/18 Pct Recovery = 61% Analysis Date = 02/11/18 Pct Recovery = 61% Analysis Date = 02/01/18 Pct Recovery = 61% Analysis Date = 02/01/18 Pct Recovery = 61% Analysis Date = 01/22/18 Pct Recovery = 61% Analysis Date = 01/22/18 Pct Recovery = 61% Analysis Date = 01/12/18 Pct Recovery = 61% Analysis Date = 01/12/18 Pct Recovery = 61% Analysis Date = 01/02/18 Pct Recovery = 61% Analysis Date = 01/02/18 Pct Recovery = 61% Analysis Date = 12/23/17 Pct Recovery = 61% Analysis Date = 12/23/17 Pct Recovery = 61% Analysis Date = 12/13/17 Pct Recovery = 61% Analysis Date = 12/13/17 Pct Recovery = 61% Analysis Date = 12/04/17 Pct Recovery = 61% Analysis Date = 12/04/17 Pct Recovery = 61% Analysis Date = 11/24/17 Pct Recovery = 62% Analysis Date = 11/24/17 Pct Recovery = 62% Analysis Date = 11/14/17 Pct Recovery = 62% Analysis Date = 11/14/17 Pct Recovery = 62% Analysis Date = 11/04/17 Pct Recovery = 62% Analysis Date = 11/04/17 Pct Recovery = 62% Analysis Date = 10/25/17 Pct Recovery = 62% Analysis Date = 10/25/17 Pct Recovery = 62% Analysis Date = 10/15/17 Pct Recovery = 62% Analysis Date = 10/15/17 Pct Recovery = 62% Analysis Date = 10/05/17 Pct Recovery = 62% Analysis Date = 10/05/17 Pct Recovery = 62% Analysis Date = 09/25/17 Pct Recovery = 62% Analysis Date = 09/25/17 Pct Recovery = 62% Analysis Date = 09/15/17 Pct Recovery = 62% Analysis Date = 09/15/17 Pct Recovery = 62% Analysis Date = 09/05/17 Pct Recovery = 62% Analysis Date = 09/05/17 Pct Recovery = 62% Analysis Date = 08/27/17 Pct Recovery = 62% Analysis Date = 08/27/17 Pct Recovery = 62% Analysis Date = 08/17/17 Pct Recovery = 62% Analysis Date = 08/17/17 Pct Recovery = 62% Analysis Date = 08/07/17 Pct Recovery = 63% Analysis Date = 08/07/17 Pct Recovery = 63% Analysis Date = 07/28/17 Pct Recovery = 63% Analysis Date = 07/28/17 Pct Recovery = 63% Analysis Date = 07/18/17 Pct Recovery = 63% Analysis Date = 07/18/17 Pct Recovery = 63% Analysis Date = 07/08/17 Pct Recovery = 63% Analysis Date = 07/08/17 Pct Recovery = 63% Analysis Date = 06/28/17 Pct Recovery = 63% Analysis Date = 06/28/17 Pct Recovery = 63% Analysis Date = 06/18/17 Pct Recovery = 63% Analysis Date = 06/18/17 Pct Recovery = 63% Analysis Date = 06/08/17 Pct Recovery = 63% Analysis Date = 06/08/17 Pct Recovery = 63% Analysis Date = 05/29/17 Pct Recovery = 63% Analysis Date = 05/29/17 Pct Recovery = 63% Analysis Date = 05/20/17 Pct Recovery = 63% Analysis Date = 05/20/17 Pct Recovery = 63% Analysis Date = 05/10/17 Pct Recovery = 63% Analysis Date = 05/10/17 Pct Recovery = 63% Analysis Date = 04/30/17 Pct Recovery = 64% Analysis Date = 04/30/17 Pct Recovery = 64% Analysis Date = 04/20/17 Pct Recovery = 64% Analysis Date = 04/20/17 Pct Recovery = 64% Analysis Date = 04/10/17 Pct Recovery = 64% Analysis Date = 04/10/17 Pct Recovery = 64% Analysis Date = 03/31/17 Pct Recovery = 64% Analysis Date = 03/31/17 Pct Recovery = 64% Analysis Date = 03/21/17 Pct Recovery = 64% Analysis Date = 03/21/17 Pct Recovery = 64% Analysis Date = 03/11/17 Pct Recovery = 64% Analysis Date = 03/11/17 Pct Recovery = 64% Analysis Date = 03/01/17 Pct Recovery = 64% Analysis Date = 03/01/17 Pct Recovery = 64% Analysis Date = 02/19/17 Pct Recovery = 64% Analysis Date = 02/19/17 Pct Recovery = 64% Analysis Date = 02/10/17 Pct Recovery = 64% Analysis Date = 02/10/17 Pct Recovery = 64% Analysis Date = 01/31/17 Pct Recovery = 65% Analysis Date = 01/31/17 Pct Recovery = 65% Analysis Date = 01/21/17 Pct Recovery = 65% Analysis Date = 01/21/17 Pct Recovery = 65% Analysis Date = 01/11/17 Pct Recovery = 65% Analysis Date = 01/11/17 Pct Recovery = 65% Analysis Date = 01/01/17 Pct Recovery = 65% Analysis Date = 01/01/17 Pct Recovery = 65% Analysis Date = 12/22/16 Pct Recovery = 65% Analysis Date = 12/22/16 Pct Recovery = 65% Analysis Date = 12/12/16 Pct Recovery = 65% Analysis Date = 12/12/16 Pct Recovery = 65% Analysis Date = 12/02/16 Pct Recovery = 65% Analysis Date = 12/02/16 Pct Recovery = 65% Analysis Date = 11/22/16 Pct Recovery = 65% Analysis Date = 11/22/16 Pct Recovery = 65% Analysis Date = 11/12/16 Pct Recovery = 66% Analysis Date = 11/12/16 Pct Recovery = 66% Analysis Date = 11/03/16 Pct Recovery = 66% Analysis Date = 11/03/16 Pct Recovery = 66% Analysis Date = 10/24/16 Pct Recovery = 66% Analysis Date = 10/24/16 Pct Recovery = 66% Analysis Date = 10/14/16 Pct Recovery = 66% Analysis Date = 10/14/16 Pct Recovery = 66% Analysis Date = 10/04/16 Pct Recovery = 66% Analysis Date = 10/04/16 Pct Recovery = 66% Analysis Date = 09/24/16 Pct Recovery = 66% Analysis Date = 09/24/16 Pct Recovery = 66% Analysis Date = 09/14/16 Pct Recovery = 66% Analysis Date = 09/14/16 Pct Recovery = 66% Analysis Date = 09/04/16 Pct Recovery = 66% Analysis Date = 09/04/16 Pct Recovery = 66% Analysis Date = 08/25/16 Pct Recovery = 67% Analysis Date = 08/25/16 Pct Recovery = 67% Analysis Date = 08/15/16 Pct Recovery = 67% Analysis Date = 08/15/16 Pct Recovery = 67% Analysis Date = 08/05/16 Pct Recovery = 67% Analysis Date = 08/05/16 Pct Recovery = 67% Analysis Date = 07/27/16 Pct Recovery = 67% Analysis Date = 07/27/16 Pct Recovery = 67% Analysis Date = 07/17/16 Pct Recovery = 67% Analysis Date = 07/17/16 Pct Recovery = 67% Analysis Date = 07/07/16 Pct Recovery = 67% Analysis Date = 07/07/16 Pct Recovery = 67% Analysis Date = 06/27/16 Pct Recovery = 68% Analysis Date = 06/27/16 Pct Recovery = 68% Analysis Date = 06/17/16 Pct Recovery = 68% Analysis Date = 06/17/16 Pct Recovery = 68% Analysis Date = 06/07/16 Pct Recovery = 68% Analysis Date = 06/07/16 Pct Recovery = 68% Analysis Date = 05/28/16 Pct Recovery = 68% Analysis Date = 05/28/16 Pct Recovery = 68% Analysis Date = 05/18/16 Pct Recovery = 68% Analysis Date = 05/18/16 Pct Recovery = 68% Analysis Date = 05/08/16 Pct Recovery = 68% Analysis Date = 05/08/16 Pct Recovery = 68% Analysis Date = 04/28/16 Pct Recovery = 69% Analysis Date = 04/28/16 Pct Recovery = 69% Analysis Date = 04/19/16 Pct Recovery = 69% Analysis Date = 04/19/16 Pct Recovery = 69% Analysis Date = 04/09/16 Pct Recovery = 69% Analysis Date = 04/09/16 Pct Recovery = 69% Analysis Date = 03/30/16 Pct Recovery = 69% Analysis Date = 03/30/16 Pct Recovery = 69% Analysis Date = 03/20/16 Pct Recovery = 69% Analysis Date = 03/20/16 Pct Recovery = 69% Analysis Date = 03/10/16 Pct Recovery = 69% Analysis Date = 03/10/16 Pct Recovery = 69% Analysis Date = 02/29/16 Pct Recovery = 70% Analysis Date = 02/29/16 Pct Recovery = 70% Analysis Date = 02/19/16 Pct Recovery = 70% Analysis Date = 02/19/16 Pct Recovery = 70% Analysis Date = 02/09/16 Pct Recovery = 70% Analysis Date = 02/09/16 Pct Recovery = 70% Analysis Date = 01/30/16 Pct Recovery = 70% Analysis Date = 01/30/16 Pct Recovery = 70% Analysis Date = 01/20/16 Pct Recovery = 70% Analysis Date = 01/20/16 Pct Recovery = 70% Analysis Date = 01/11/16 Pct Recovery = 70% Analysis Date = 01/11/16 Pct Recovery = 70% Analysis Date = 01/01/16 Pct Recovery = 70% Analysis Date = 01/01/16 Pct Recovery = 70% Analysis Date = 12/22/15 Pct Recovery = 70% Analysis Date = 12/22/15 Pct Recovery = 70% Analysis Date = 12/12/15 Pct Recovery = 70% Analysis Date = 12/12/15 Pct Recovery = 70% Analysis Date = 12/02/15 Pct Recovery = 70% Analysis Date = 12/02/15 Pct Recovery = 70% Analysis Date = 11/22/15 Pct Recovery = 70% Analysis Date = 11/22/15 Pct Recovery = 70% Analysis Date = 11/12/15 Pct Recovery = 70% Analysis Date = 11/12/15 Pct Recovery = 70% Analysis Date = 11/02/15 Pct Recovery = 70% Analysis Date = 11/02/15 Pct Recovery = 70% Analysis Date = 10/23/15 Pct Recovery = 70% Analysis Date = 10/23/15 Pct Recovery = 70% Analysis Date = 10/13/15 Pct Recovery = 70% Analysis Date = 10/13/15 Pct Recovery = 70% Analysis Date = 10/04/15 Pct Recovery = 70% Analysis Date = 10/04/15 Pct Recovery = 70% Analysis Date = 09/24/15 Pct Recovery = 70% Analysis Date = 09/24/15 Pct Recovery = 70% Analysis Date = 09/14/15 Pct Recovery = 70% Analysis Date = 09/14/15 Pct Recovery = 70% Analysis Date = 09/04/15 Pct Recovery = 70% Analysis Date = 09/04/15 Pct Recovery = 70% Analysis Date = 08/25/15 Pct Recovery = 70% Analysis Date = 08/25/15 Pct Recovery = 70% Analysis Date = 08/15/15 Pct Recovery = 70% Analysis Date = 08/15/15 Pct Recovery = 70% Analysis Date = 08/05/15 Pct Recovery = 70% Analysis Date = 08/05/15 Pct Recovery = 70% Analysis Date = 07/26/15 Pct Recovery = 70% Analysis Date = 07/26/15 Pct Recovery = 70% Analysis Date = 07/16/15 Pct Recovery = 70% Analysis Date = 07/16/15 Pct Recovery = 70% Analysis Date = 07/06/15 Pct Recovery = 70% Analysis Date = 07/06/15 Pct Recovery = 70% Analysis Date = 06/27/15 Pct Recovery = 70% Analysis Date = 06/27/15 Pct Recovery = 70% Analysis Date = 06/17/15 Pct Recovery = 70% Analysis Date = 06/17/15 Pct Recovery = 70% Analysis Date = 06/07/15 Pct Recovery = 70% Analysis Date = 06/07/15 Pct Recovery = 70% Analysis Date = 05/28/15 Pct Recovery = 70% Analysis Date = 05/28/15 Pct Recovery = 70% Analysis Date = 05/18/15 Pct Recovery = 70% Analysis Date = 05/18/15 Pct Recovery = 70% Analysis Date = 05/08/15 Pct Recovery = 70% Analysis Date = 05/08/15 Pct Recovery = 70% Analysis Date = 04/28/15 Pct Recovery = 69% Analysis Date = 04/28/15 Pct Recovery = 69% Analysis Date = 04/18/15 Pct Recovery = 69% Analysis Date = 04/18/15 Pct Recovery = 69% Analysis Date = 04/08/15 Pct Recovery = 69% Analysis Date = 04/08/15 Pct Recovery = 69% Analysis Date = 03/29/15 Pct Recovery = 69% Analysis Date = 03/29/15 Pct Recovery = 69% Analysis Date = 03/20/15 Pct Recovery = 69% Analysis Date = 03/20/15 Pct Recovery = 69% Analysis Date = 03/10/15 Pct Recovery = 69% Analysis Date = 03/10/15 Pct Recovery = 69% Analysis Date = 02/28/15 Pct Recovery = 69% Analysis Date = 02/28/15 Pct Recovery = 69% Analysis Date = 02/18/15 Pct Recovery = 69% Analysis Date = 02/18/15 Pct Recovery = 69% Analysis Date = 02/08/15 Pct Recovery = 68% Analysis Date = 02/08/15 Pct Recovery = 68% Analysis Date = 01/29/15 Pct Recovery = 68% Analysis Date = 01/29/15 Pct Recovery = 68% Analysis Date = 01/19/15 Pct Recovery = 68% Analysis Date = 01/19/15 Pct Recovery = 68% Analysis Date = 01/09/15 Pct Recovery = 68% Analysis Date = 01/09/15 Pct Recovery = 68% Analysis Date = 12/30/14 Pct Recovery = 68% Analysis Date = 12/30/14 Pct Recovery = 68% Analysis Date = 12/20/14 Pct Recovery = 68% Analysis Date = 12/20/14 Pct Recovery = 68% Analysis Date = 12/11/14 Pct Recovery = 68% Analysis Date = 12/11/14 Pct Recovery = 68% Analysis Date = 12/01/14 Pct Recovery = 68% Analysis Date = 12/01/14 Pct Recovery = 68% Analysis Date = 11/21/14 Pct Recovery = 67% Analysis Date = 11/21/14 Pct Recovery = 67% Analysis Date = 11/11/14 Pct Recovery = 67% Analysis Date = 11/11/14 Pct Recovery = 67% Analysis Date = 11/01/14 Pct Recovery = 67% Analysis Date = 11/01/14 Pct Recovery = 67% Analysis Date = 10/22/14 Pct Recovery = 67% Analysis Date = 10/22/14 Pct Recovery = 67% Analysis Date = 10/12/14 Pct Recovery = 67% Analysis Date = 10/12/14 Pct Recovery = 67% Analysis Date = 10/02/14 Pct Recovery = 66% Analysis Date = 10/02/14 Pct Recovery = 66% Analysis Date = 09/22/14 Pct Recovery = 66% Analysis Date = 09/22/14 Pct Recovery = 66% Analysis Date = 09/12/14 Pct Recovery = 66% Analysis Date = 09/12/14 Pct Recovery = 66% Analysis Date = 09/03/14 Pct Recovery = 65% Analysis Date = 09/03/14 Pct Recovery = 65% Analysis Date = 08/24/14 Pct Recovery = 65% Analysis Date = 08/24/14 Pct Recovery = 65% Analysis Date = 08/14/14 Pct Recovery = 65% Analysis Date = 08/14/14 Pct Recovery = 65% Analysis Date = 08/04/14 Pct Recovery = 64% Analysis Date = 08/04/14 Pct Recovery = 64% Analysis Date = 07/25/14 Pct Recovery = 64% Analysis Date = 07/25/14 Pct Recovery = 64% Analysis Date = 07/15/14 Pct Recovery = 64% Analysis Date = 07/15/14 Pct Recovery = 64% Analysis Date = 07/05/14 Pct Recovery = 63% Analysis Date = 07/05/14 Pct Recovery = 63% Analysis Date = 06/25/14 Pct Recovery = 63% Analysis Date = 06/25/14 Pct Recovery = 63% Analysis Date = 06/15/14 Pct Recovery = 62% Analysis Date = 06/15/14 Pct Recovery = 62% Analysis Date = 06/05/14 Pct Recovery = 62% Analysis Date = 06/05/14 Pct Recovery = 62% Analysis Date = 05/27/14 Pct Recovery = 61% Analysis Date = 05/27/14 Pct Recovery = 61% Analysis Date = 05/17/14 Pct Recovery = 61% Analysis Date = 05/17/14 Pct Recovery = 61% Analysis Date = 05/07/14 Pct Recovery = 62% Analysis Date = 05/07/14 Pct Recovery = 62% Analysis Date = 04/27/14 Pct Recovery = 62% Analysis Date = 04/27/14 Pct Recovery = 62% Analysis Date = 04/17/14 Pct Recovery = 62% Analysis Date = 04/17/14 Pct Recovery = 62% Analysis Date = 04/07/14 Pct Recovery = 62% Analysis Date = 04/07/14 Pct Recovery = 62% Analysis Date = 03/28/14 Pct Recovery = 62% Analysis Date = 03/28/14 Pct Recovery = 62% Analysis Date = 03/18/14 Pct Recovery = 62% Analysis Date = 03/18/14 Pct Recovery = 62% Analysis Date = 03/08/14 Pct Recovery = 62% Analysis Date = 03/08/14 Pct Recovery = 62% Analysis Date = 02/26/14 Pct Recovery = 62% Analysis Date = 02/26/14 Pct Recovery = 62% Analysis Date = 02/17/14 Pct Recovery = 62% Analysis Date = 02/17/14 Pct Recovery = 62% Analysis Date = 02/07/14 Pct Recovery = 62% Analysis Date = 02/07/14 Pct Recovery = 62% Analysis Date = 01/28/14 Pct Recovery = 62% Analysis Date = 01/28/14 Pct Recovery = 62% Analysis Date = 01/18/14 Pct Recovery = 62% Analysis Date = 01/18/14 Pct Recovery = 62% Analysis Date = 01/08/14 Pct Recovery = 62% Analysis Date = 01/08/14 Pct Recovery = 62% Analysis Date = 12/29/13 Pct Recovery = 63% Analysis Date = 12/29/13 Pct Recovery = 63% Analysis Date = 12/19/13 Pct Recovery = 63% Analysis Date = 12/19/13 Pct Recovery = 63% Analysis Date = 12/09/13 Pct Recovery = 63% Analysis Date = 12/09/13 Pct Recovery = 63% Analysis Date = 11/29/13 Pct Recovery = 63% Analysis Date = 11/29/13 Pct Recovery = 63% Analysis Date = 11/19/13 Pct Recovery = 63% Analysis Date = 11/19/13 Pct Recovery = 63% Analysis Date = 11/10/13 Pct Recovery = 63% Analysis Date = 11/10/13 Pct Recovery = 63% Analysis Date = 10/31/13 Pct Recovery = 64% Analysis Date = 10/31/13 Pct Recovery = 64% Analysis Date = 10/21/13 Pct Recovery = 64% Analysis Date = 10/21/13 Pct Recovery = 64% Analysis Date = 10/11/13 Pct Recovery = 64% Analysis Date = 10/11/13 Pct Recovery = 64% Analysis Date = 10/01/13 Pct Recovery = 64% Analysis Date = 10/01/13 Pct Recovery = 64% Analysis Date = 09/21/13 Pct Recovery = 64% Analysis Date = 09/21/13 Pct Recovery = 64% Analysis Date = 09/11/13 Pct Recovery = 65% Analysis Date = 09/11/13 Pct Recovery = 65% Analysis Date = 09/01/13 Pct Recovery = 65% Analysis Date = 09/01/13 Pct Recovery = 65% Analysis Date = 08/22/13 Pct Recovery = 65% Analysis Date = 08/22/13 Pct Recovery = 65% Analysis Date = 08/12/13 Pct Recovery = 65% Analysis Date = 08/12/13 Pct Recovery = 65% Analysis Date = 08/03/13 Pct Recovery = 65% Analysis Date = 08/03/13 Pct Recovery = 65% Analysis Date = 07/24/13 Pct Recovery = 66% Analysis Date = 07/24/13 Pct Recovery = 66% Analysis Date = 07/14/13 Pct Recovery = 66% Analysis Date = 07/14/13 Pct Recovery = 66% Analysis Date = 07/04/13 Pct Recovery = 66% Analysis Date = 07/04/13 Pct Recovery = 66% Analysis Date = 06/24/13 Pct Recovery = 66% Analysis Date = 06/24/13 Pct Recovery = 66% Analysis Date = 06/14/13 Pct Recovery = 66% Analysis Date = 06/14/13 Pct Recovery = 66% Analysis Date = 06/04/13 Pct Recovery = 67% Analysis Date = 06/04/13 Pct Recovery = 67% Analysis Date = 05/25/13 Pct Recovery = 67% Analysis Date = 05/25/13 Pct Recovery = 67% Analysis Date = 05/15/13 Pct Recovery = 67% Analysis Date = 05/15/13 Pct Recovery = 67% Analysis Date = 05/05/13 Pct Recovery = 67% Analysis Date = 05/05/13 Pct Recovery = 67% Analysis Date = 04/26/13 Pct Recovery = 67% Analysis Date = 04/26/13 Pct Recovery = 67% Analysis Date = 04/16/13 Pct Recovery = 68% Analysis Date = 04/16/13 Pct Recovery = 68% Analysis Date = 04/06/13 Pct Recovery = 68% Analysis Date = 04/06/13 Pct Recovery = 68% Analysis Date = 03/27/13 Pct Recovery = 68% Analysis Date = 03/27/13 Pct Recovery = 68% Analysis Date = 03/17/13 Pct Recovery = 68% Analysis Date = 03/17/13 Pct Recovery = 68% Analysis Date = 03/07/13 Pct Recovery = 69% Analysis Date = 03/07/13 Pct Recovery = 69% Analysis Date = 02/25/13 Pct Recovery = 69% Analysis Date = 02/25/13 Pct Recovery = 69% Analysis Date = 02/15/13 Pct Recovery = 69% Analysis Date = 02/15/13 Pct Recovery = 69% Analysis Date = 02/05/13 Pct Recovery = 69% Analysis Date = 02/05/13 Pct Recovery = 69% Analysis Date = 01/26/13 Pct Recovery = 69% Analysis Date = 01/26/13 Pct Recovery = 69% Analysis Date = 01/17/13 Pct Recovery = 70% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
TEBUCONAZOLE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 79 65% 15% 64% 14%
Total 79 65% 15% 64% 14%

Sample Statistics
TEBUCONAZOLE

Characteristic N % % Basis
Plotted 79 100% Spiked
Estimated Values 3 4% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 79 .  
False Negatives 0 0% 0 out of 79
Not Spiked 55 .  
False Positives 0 0% 0 out of 55

OBSP Determination:
TEBUTHIURON
METHOD: 2033 , TESTIDCODE: 82670GCM35

Laboratory ID = 20161470001 Lab Value = 0.341 Expected Conc. = 0.14 Report level label = 0.028 Pct Recovery = 244% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl SpecificMix = LC20138V Laboratory ID = 20162520001 Lab Value = 0.158 Expected Conc. = 0.07 Report level label = 0.028 Pct Recovery = 226% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl SpecificMix = LC20138V Laboratory ID = 20131920149 Lab Value = 0.124 Expected Conc. = 0.0606 Report level label = 0.028 Pct Recovery = 205% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl SpecificMix = 012513 Laboratory ID = 20140100085 Lab Value = 0.510 Expected Conc. = 0.401 Report level label = 0.028 Pct Recovery = 127% Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl SpecificMix = 042413 Laboratory ID = 20130250061 Lab Value = 0.270 Expected Conc. = 0.299 Report level label = 0.028 Pct Recovery = 90% Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl SpecificMix = 05BB029 Laboratory ID = 20132690010 Lab Value = 0.302 Expected Conc. = 0.2005 Report level label = 0.028 Pct Recovery = 151% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl SpecificMix = 042413 Laboratory ID = 20132560001 Lab Value = 0.282 Expected Conc. = 0.2005 Report level label = 0.028 Pct Recovery = 141% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl SpecificMix = 042413 Laboratory ID = 20132140002 Lab Value = 0.314 Expected Conc. = 0.199 Report level label = 0.028 Pct Recovery = 158% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl SpecificMix = 04CC101 Laboratory ID = 20172510330 Lab Value = 0.195 Expected Conc. = 0.187 Report level label = 0.028 Pct Recovery = 104% Analysis Date = 12/29/17 SpikeMix = ChemService 6537100: 100 µl & Abs 071817Pest: 100 µl SpecificMix = 071817Pest Laboratory ID = 20162860079 Lab Value = 0.177 Expected Conc. = 0.18 Report level label = 0.028 Pct Recovery = 98% Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl SpecificMix = 5054800 Laboratory ID = 20161880109 Lab Value = 0.255 Expected Conc. = 0.18 Report level label = 0.028 Pct Recovery = 142% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl SpecificMix = 5054800 Laboratory ID = 20163370001 Lab Value = 0.183 Expected Conc. = 0.175 Report level label = 0.028 Pct Recovery = 105% Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl SpecificMix = LC20138V Laboratory ID = 20152610011 Lab Value = 0.118 Expected Conc. = 0.1664 Report level label = 0.028 Pct Recovery = 71% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl SpecificMix = 0406-15-01 Laboratory ID = 20152460215 Lab Value = 0.204 Expected Conc. = 0.1664 Report level label = 0.028 Pct Recovery = 123% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl SpecificMix = 0406-15-01 Laboratory ID = 20140230082 Lab Value = 0.126 Expected Conc. = 0.1515 Report level label = 0.028 Pct Recovery = 83% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl SpecificMix = 012513 Laboratory ID = 20132420001 Lab Value = 0.183 Expected Conc. = 0.1515 Report level label = 0.028 Pct Recovery = 121% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl SpecificMix = 012513 Laboratory ID = 20130940097 Lab Value = 0.143 Expected Conc. = 0.1515 Report level label = 0.028 Pct Recovery = 94% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = 052412 Laboratory ID = 20130100066 Lab Value = 0.170 Expected Conc. = 0.1515 Report level label = 0.028 Pct Recovery = 112% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl SpecificMix = 052412 Laboratory ID = 20171380001 Lab Value = 0.095 Expected Conc. = 0.144 Report level label = 0.028 Pct Recovery = 66% Analysis Date = 06/07/17 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 5054800 Laboratory ID = 20170960001 Lab Value = 0.151 Expected Conc. = 0.144 Report level label = 0.028 Pct Recovery = 105% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl SpecificMix = 5054800 Laboratory ID = 20161740258 Lab Value = 0.186 Expected Conc. = 0.144 Report level label = 0.028 Pct Recovery = 129% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 5054800 Laboratory ID = 20171720140 Lab Value = 0.229 Expected Conc. = 0.14 Report level label = 0.028 Pct Recovery = 164% Analysis Date = 08/31/17 SpikeMix = Supelco LC20138V: 80 µl & Phenova B20160331: 80 µl SpecificMix = LC20138V Laboratory ID = 20170740063 Lab Value = 0.103 Expected Conc. = 0.14 Report level label = 0.028 Pct Recovery = 74% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl SpecificMix = LC20138V Laboratory ID = 20150720069 Lab Value = 0.078 Expected Conc. = 0.1122 Report level label = 0.028 Pct Recovery = 70% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 0227-14-08 Laboratory ID = 20141770149 Lab Value = 0.113 Expected Conc. = 0.1122 Report level label = 0.028 Pct Recovery = 101% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl SpecificMix = 0227-14-08 Laboratory ID = 20141570088 Lab Value = 0.194 Expected Conc. = 0.1122 Report level label = 0.028 Pct Recovery = 173% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl SpecificMix = 0227-14-08 Laboratory ID = 20150430092 Lab Value = 0.067 Expected Conc. = 0.1116 Report level label = 0.028 Pct Recovery = 60% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl SpecificMix = 042814 Laboratory ID = 20143240095 Lab Value = 0.140 Expected Conc. = 0.1116 Report level label = 0.028 Pct Recovery = 125% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl SpecificMix = 042814 Laboratory ID = 20142960086 Lab Value = 0.106 Expected Conc. = 0.1116 Report level label = 0.028 Pct Recovery = 95% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 042814 Laboratory ID = 20142530087 Lab Value = 0.087 Expected Conc. = 0.1116 Report level label = 0.028 Pct Recovery = 78% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl SpecificMix = 042814 Laboratory ID = 20173480003 Lab Value = 0.087 Expected Conc. = 0.095 Report level label = 0.028 Pct Recovery = 92% Analysis Date = 04/05/18 SpikeMix = Abs 071717Pest: 50 µl & ChemService 6567600: 50 µl SpecificMix = 6567600 Laboratory ID = 20172560101 Lab Value = 0.114 Expected Conc. = 0.095 Report level label = 0.028 Pct Recovery = 120% Analysis Date = 12/22/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6567600: 50 µl SpecificMix = 6567600 Laboratory ID = 20181430122 Lab Value = 0.145 Expected Conc. = 0.0935 Report level label = 0.028 Pct Recovery = 155% Analysis Date = 06/20/18 SpikeMix = Abs 071817Pest: 50 µl & Spex Organics EN170808006: 50 µl SpecificMix = 071817Pest Laboratory ID = 20161260151 Lab Value = 0.106 Expected Conc. = 0.084 Report level label = 0.028 Pct Recovery = 126% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = 3851600 Laboratory ID = 20151550293 Lab Value = 0.135 Expected Conc. = 0.084 Report level label = 0.028 Pct Recovery = 161% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl SpecificMix = 3851600 Laboratory ID = 20151270112 Lab Value = 0.088 Expected Conc. = 0.084 Report level label = 0.028 Pct Recovery = 105% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl SpecificMix = 3851600 Laboratory ID = 20160770090 Lab Value = 0.091 Expected Conc. = 0.0832 Report level label = 0.028 Pct Recovery = 110% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20160630046 Lab Value = 0.102 Expected Conc. = 0.0832 Report level label = 0.028 Pct Recovery = 123% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20153510109 Lab Value = 0.053 Expected Conc. = 0.0832 Report level label = 0.028 Pct Recovery = 64% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20153440001 Lab Value = 0.055 Expected Conc. = 0.0832 Report level label = 0.028 Pct Recovery = 67% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20133580036 Lab Value = 0.058 Expected Conc. = 0.0802 Report level label = 0.028 Pct Recovery = 72% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 042413 Laboratory ID = 20133190012 Lab Value = 0.096 Expected Conc. = 0.0802 Report level label = 0.028 Pct Recovery = 120% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 042413 Laboratory ID = 20131650073 Lab Value = 0.157 Expected Conc. = 0.0802 Report level label = 0.028 Pct Recovery = 196% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl SpecificMix = 042413 Laboratory ID = 20140730138 Lab Value = 0.057 Expected Conc. = 0.0796 Report level label = 0.028 Pct Recovery = 72% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 04CC101 Laboratory ID = 20140510043 Lab Value = 0.064 Expected Conc. = 0.0796 Report level label = 0.028 Pct Recovery = 80% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 04CC101 Laboratory ID = 20133310030 Lab Value = 0.096 Expected Conc. = 0.0796 Report level label = 0.028 Pct Recovery = 120% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl SpecificMix = 04CC101 Laboratory ID = 20132280016 Lab Value = 0.130 Expected Conc. = 0.0796 Report level label = 0.028 Pct Recovery = 163% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl SpecificMix = 04CC101 Laboratory ID = 20131510026 Lab Value = 0.105 Expected Conc. = 0.0796 Report level label = 0.028 Pct Recovery = 132% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl SpecificMix = 04CC101 Laboratory ID = 20171940002 Lab Value = 0.096 Expected Conc. = 0.072 Report level label = 0.028 Pct Recovery = 134% Analysis Date = 11/10/17 SpikeMix = ChemService 5054800: 40 µl & NSI 041816: 40 µl SpecificMix = 5054800 Laboratory ID = 20170460061 Lab Value = 0.089 Expected Conc. = 0.072 Report level label = 0.028 Pct Recovery = 124% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl SpecificMix = 5054800 Laboratory ID = 20163560019 Lab Value = 0.074 Expected Conc. = 0.072 Report level label = 0.028 Pct Recovery = 103% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl SpecificMix = 5054800 Laboratory ID = 20162150213 Lab Value = 0.082 Expected Conc. = 0.072 Report level label = 0.028 Pct Recovery = 114% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl SpecificMix = 5054800 Laboratory ID = 20171510080 Lab Value = 0.082 Expected Conc. = 0.07 Report level label = 0.028 Pct Recovery = 117% Analysis Date = 06/09/17 SpikeMix = Supelco LC20138V: 40 µl & Crescent 03FF076: 40 µl SpecificMix = LC20138V Laboratory ID = 20162660005 Lab Value = 0.076 Expected Conc. = 0.07 Report level label = 0.028 Pct Recovery = 109% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl SpecificMix = LC20138V Laboratory ID = 20162020124 Lab Value = 0.069 Expected Conc. = 0.07 Report level label = 0.028 Pct Recovery = 99% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl SpecificMix = LC20138V Laboratory ID = 20140860102 Lab Value = 0.077 Expected Conc. = 0.0606 Report level label = 0.028 Pct Recovery = 127% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 012513 Laboratory ID = 20133400002 Lab Value = 0.065 Expected Conc. = 0.0606 Report level label = 0.028 Pct Recovery = 107% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = 052412 Laboratory ID = 20132910008 Lab Value = 0.091 Expected Conc. = 0.0606 Report level label = 0.028 Pct Recovery = 150% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = 052412 Laboratory ID = 20131920149 Lab Value = 0.124 Expected Conc. = 0.0606 Report level label = 0.028 Pct Recovery = 205% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl SpecificMix = 012513 Laboratory ID = 20130650005 Lab Value = 0.069 Expected Conc. = 0.0606 Report level label = 0.028 Pct Recovery = 114% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl SpecificMix = 052412 Laboratory ID = 20131230084 Lab Value = 0.104 Expected Conc. = 0.0598 Report level label = 0.028 Pct Recovery = 174% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl SpecificMix = 05BB029 Laboratory ID = 20130510051 Lab Value = 0.064 Expected Conc. = 0.0598 Report level label = 0.028 Pct Recovery = 106% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl SpecificMix = 05BB029 Laboratory ID = 20180730064 Lab Value = 0.107 Expected Conc. = 0.0561 Report level label = 0.028 Pct Recovery = 191% Analysis Date = 05/16/18 SpikeMix = Abs 071717Pest: 30 µl & Abs 071817Pest: 30 µl SpecificMix = 071817Pest Laboratory ID = 20180050004 Lab Value = 0.073 Expected Conc. = 0.0561 Report level label = 0.028 Pct Recovery = 130% Analysis Date = 04/05/18 SpikeMix = Abs 071817Pest: 30 µl & ChemService 6472100: 30 µl SpecificMix = 071817Pest Laboratory ID = 20172780018 Lab Value = 0.053 Expected Conc. = 0.0561 Report level label = 0.028 Pct Recovery = 95% Analysis Date = 02/08/18 SpikeMix = ChemService 6537100: 30 µl & Abs 071817Pest: 30 µl SpecificMix = 071817Pest Laboratory ID = 20141840097 Lab Value = 0.060 Expected Conc. = 0.0561 Report level label = 0.028 Pct Recovery = 106% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20141490205 Lab Value = 0.085 Expected Conc. = 0.0561 Report level label = 0.028 Pct Recovery = 152% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20141420140 Lab Value = 0.036 Expected Conc. = 0.0561 Report level label = 0.028 Pct Recovery = 65% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20141360094 Lab Value = 0.054 Expected Conc. = 0.0561 Report level label = 0.028 Pct Recovery = 96% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20143370094 Lab Value = 0.064 Expected Conc. = 0.0558 Report level label = 0.028 Pct Recovery = 114% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl SpecificMix = 042814 Laboratory ID = 20142820151 Lab Value = 0.067 Expected Conc. = 0.0558 Report level label = 0.028 Pct Recovery = 121% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl SpecificMix = 042814 Laboratory ID = 20142470041 Lab Value = 0.068 Expected Conc. = 0.0558 Report level label = 0.028 Pct Recovery = 121% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl SpecificMix = 042814 Laboratory ID = 20142200164 Lab Value = 0.079 Expected Conc. = 0.0558 Report level label = 0.028 Pct Recovery = 142% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 042814 Laboratory ID = 20160430111 Lab Value = 0.055 Expected Conc. = 0.042 Report level label = 0.028 Pct Recovery = 131% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 3851600 Laboratory ID = 20160210080 Lab Value = 0.052 Expected Conc. = 0.042 Report level label = 0.028 Pct Recovery = 124% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 3851600 Laboratory ID = 20152950078 Lab Value = 0.024 Expected Conc. = 0.042 Report level label = 0.028 Pct Recovery = 56% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 3851600 Laboratory ID = 20153030068 Lab Value = 0.044 Expected Conc. = 0.042 Report level label = 0.028 Pct Recovery = 105% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = 3851600 Laboratory ID = 20151760208 Lab Value = 0.060 Expected Conc. = 0.042 Report level label = 0.028 Pct Recovery = 143% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl SpecificMix = 3851600 Laboratory ID = 20151380009 Lab Value = 0.056 Expected Conc. = 0.042 Report level label = 0.028 Pct Recovery = 133% Analysis Date = 05/30/15 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 3851600 Laboratory ID = 20152190003 Lab Value = 0.045 Expected Conc. = 0.0416 Report level label = 0.028 Pct Recovery = 107% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = 0406-15-01 Laboratory ID = 20152040177 Lab Value = 0.053 Expected Conc. = 0.0416 Report level label = 0.028 Pct Recovery = 127% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl SpecificMix = 0406-15-01 Analysis Date = 06/20/18 Pct Recovery = 131% Analysis Date = 06/10/18 Pct Recovery = 131% Analysis Date = 06/10/18 Pct Recovery = 131% Analysis Date = 05/31/18 Pct Recovery = 131% Analysis Date = 05/31/18 Pct Recovery = 131% Analysis Date = 05/21/18 Pct Recovery = 131% Analysis Date = 05/21/18 Pct Recovery = 131% Analysis Date = 05/11/18 Pct Recovery = 131% Analysis Date = 05/11/18 Pct Recovery = 131% Analysis Date = 05/01/18 Pct Recovery = 130% Analysis Date = 05/01/18 Pct Recovery = 130% Analysis Date = 04/21/18 Pct Recovery = 130% Analysis Date = 04/21/18 Pct Recovery = 130% Analysis Date = 04/11/18 Pct Recovery = 130% Analysis Date = 04/11/18 Pct Recovery = 130% Analysis Date = 04/01/18 Pct Recovery = 130% Analysis Date = 04/01/18 Pct Recovery = 130% Analysis Date = 03/22/18 Pct Recovery = 130% Analysis Date = 03/22/18 Pct Recovery = 130% Analysis Date = 03/13/18 Pct Recovery = 129% Analysis Date = 03/13/18 Pct Recovery = 129% Analysis Date = 03/03/18 Pct Recovery = 129% Analysis Date = 03/03/18 Pct Recovery = 129% Analysis Date = 02/21/18 Pct Recovery = 129% Analysis Date = 02/21/18 Pct Recovery = 129% Analysis Date = 02/11/18 Pct Recovery = 129% Analysis Date = 02/11/18 Pct Recovery = 129% Analysis Date = 02/01/18 Pct Recovery = 129% Analysis Date = 02/01/18 Pct Recovery = 129% Analysis Date = 01/22/18 Pct Recovery = 128% Analysis Date = 01/22/18 Pct Recovery = 128% Analysis Date = 01/12/18 Pct Recovery = 128% Analysis Date = 01/12/18 Pct Recovery = 128% Analysis Date = 01/02/18 Pct Recovery = 128% Analysis Date = 01/02/18 Pct Recovery = 128% Analysis Date = 12/23/17 Pct Recovery = 128% Analysis Date = 12/23/17 Pct Recovery = 128% Analysis Date = 12/13/17 Pct Recovery = 127% Analysis Date = 12/13/17 Pct Recovery = 127% Analysis Date = 12/04/17 Pct Recovery = 127% Analysis Date = 12/04/17 Pct Recovery = 127% Analysis Date = 11/24/17 Pct Recovery = 127% Analysis Date = 11/24/17 Pct Recovery = 127% Analysis Date = 11/14/17 Pct Recovery = 127% Analysis Date = 11/14/17 Pct Recovery = 127% Analysis Date = 11/04/17 Pct Recovery = 127% Analysis Date = 11/04/17 Pct Recovery = 127% Analysis Date = 10/25/17 Pct Recovery = 126% Analysis Date = 10/25/17 Pct Recovery = 126% Analysis Date = 10/15/17 Pct Recovery = 126% Analysis Date = 10/15/17 Pct Recovery = 126% Analysis Date = 10/05/17 Pct Recovery = 126% Analysis Date = 10/05/17 Pct Recovery = 126% Analysis Date = 09/25/17 Pct Recovery = 126% Analysis Date = 09/25/17 Pct Recovery = 126% Analysis Date = 09/15/17 Pct Recovery = 125% Analysis Date = 09/15/17 Pct Recovery = 125% Analysis Date = 09/05/17 Pct Recovery = 125% Analysis Date = 09/05/17 Pct Recovery = 125% Analysis Date = 08/27/17 Pct Recovery = 125% Analysis Date = 08/27/17 Pct Recovery = 125% Analysis Date = 08/17/17 Pct Recovery = 125% Analysis Date = 08/17/17 Pct Recovery = 125% Analysis Date = 08/07/17 Pct Recovery = 125% Analysis Date = 08/07/17 Pct Recovery = 125% Analysis Date = 07/28/17 Pct Recovery = 124% Analysis Date = 07/28/17 Pct Recovery = 124% Analysis Date = 07/18/17 Pct Recovery = 124% Analysis Date = 07/18/17 Pct Recovery = 124% Analysis Date = 07/08/17 Pct Recovery = 124% Analysis Date = 07/08/17 Pct Recovery = 124% Analysis Date = 06/28/17 Pct Recovery = 124% Analysis Date = 06/28/17 Pct Recovery = 124% Analysis Date = 06/18/17 Pct Recovery = 123% Analysis Date = 06/18/17 Pct Recovery = 123% Analysis Date = 06/08/17 Pct Recovery = 123% Analysis Date = 06/08/17 Pct Recovery = 123% Analysis Date = 05/29/17 Pct Recovery = 123% Analysis Date = 05/29/17 Pct Recovery = 123% Analysis Date = 05/20/17 Pct Recovery = 123% Analysis Date = 05/20/17 Pct Recovery = 123% Analysis Date = 05/10/17 Pct Recovery = 122% Analysis Date = 05/10/17 Pct Recovery = 122% Analysis Date = 04/30/17 Pct Recovery = 122% Analysis Date = 04/30/17 Pct Recovery = 122% Analysis Date = 04/20/17 Pct Recovery = 122% Analysis Date = 04/20/17 Pct Recovery = 122% Analysis Date = 04/10/17 Pct Recovery = 122% Analysis Date = 04/10/17 Pct Recovery = 122% Analysis Date = 03/31/17 Pct Recovery = 122% Analysis Date = 03/31/17 Pct Recovery = 122% Analysis Date = 03/21/17 Pct Recovery = 121% Analysis Date = 03/21/17 Pct Recovery = 121% Analysis Date = 03/11/17 Pct Recovery = 121% Analysis Date = 03/11/17 Pct Recovery = 121% Analysis Date = 03/01/17 Pct Recovery = 121% Analysis Date = 03/01/17 Pct Recovery = 121% Analysis Date = 02/19/17 Pct Recovery = 121% Analysis Date = 02/19/17 Pct Recovery = 121% Analysis Date = 02/10/17 Pct Recovery = 120% Analysis Date = 02/10/17 Pct Recovery = 120% Analysis Date = 01/31/17 Pct Recovery = 120% Analysis Date = 01/31/17 Pct Recovery = 120% Analysis Date = 01/21/17 Pct Recovery = 120% Analysis Date = 01/21/17 Pct Recovery = 120% Analysis Date = 01/11/17 Pct Recovery = 120% Analysis Date = 01/11/17 Pct Recovery = 120% Analysis Date = 01/01/17 Pct Recovery = 119% Analysis Date = 01/01/17 Pct Recovery = 119% Analysis Date = 12/22/16 Pct Recovery = 119% Analysis Date = 12/22/16 Pct Recovery = 119% Analysis Date = 12/12/16 Pct Recovery = 119% Analysis Date = 12/12/16 Pct Recovery = 119% Analysis Date = 12/02/16 Pct Recovery = 119% Analysis Date = 12/02/16 Pct Recovery = 119% Analysis Date = 11/22/16 Pct Recovery = 119% Analysis Date = 11/22/16 Pct Recovery = 119% Analysis Date = 11/12/16 Pct Recovery = 118% Analysis Date = 11/12/16 Pct Recovery = 118% Analysis Date = 11/03/16 Pct Recovery = 118% Analysis Date = 11/03/16 Pct Recovery = 118% Analysis Date = 10/24/16 Pct Recovery = 118% Analysis Date = 10/24/16 Pct Recovery = 118% Analysis Date = 10/14/16 Pct Recovery = 118% Analysis Date = 10/14/16 Pct Recovery = 118% Analysis Date = 10/04/16 Pct Recovery = 118% Analysis Date = 10/04/16 Pct Recovery = 118% Analysis Date = 09/24/16 Pct Recovery = 117% Analysis Date = 09/24/16 Pct Recovery = 117% Analysis Date = 09/14/16 Pct Recovery = 117% Analysis Date = 09/14/16 Pct Recovery = 117% Analysis Date = 09/04/16 Pct Recovery = 117% Analysis Date = 09/04/16 Pct Recovery = 117% Analysis Date = 08/25/16 Pct Recovery = 117% Analysis Date = 08/25/16 Pct Recovery = 117% Analysis Date = 08/15/16 Pct Recovery = 117% Analysis Date = 08/15/16 Pct Recovery = 117% Analysis Date = 08/05/16 Pct Recovery = 117% Analysis Date = 08/05/16 Pct Recovery = 117% Analysis Date = 07/27/16 Pct Recovery = 116% Analysis Date = 07/27/16 Pct Recovery = 116% Analysis Date = 07/17/16 Pct Recovery = 116% Analysis Date = 07/17/16 Pct Recovery = 116% Analysis Date = 07/07/16 Pct Recovery = 116% Analysis Date = 07/07/16 Pct Recovery = 116% Analysis Date = 06/27/16 Pct Recovery = 116% Analysis Date = 06/27/16 Pct Recovery = 116% Analysis Date = 06/17/16 Pct Recovery = 116% Analysis Date = 06/17/16 Pct Recovery = 116% Analysis Date = 06/07/16 Pct Recovery = 116% Analysis Date = 06/07/16 Pct Recovery = 116% Analysis Date = 05/28/16 Pct Recovery = 116% Analysis Date = 05/28/16 Pct Recovery = 116% Analysis Date = 05/18/16 Pct Recovery = 116% Analysis Date = 05/18/16 Pct Recovery = 116% Analysis Date = 05/08/16 Pct Recovery = 115% Analysis Date = 05/08/16 Pct Recovery = 115% Analysis Date = 04/28/16 Pct Recovery = 115% Analysis Date = 04/28/16 Pct Recovery = 115% Analysis Date = 04/19/16 Pct Recovery = 115% Analysis Date = 04/19/16 Pct Recovery = 115% Analysis Date = 04/09/16 Pct Recovery = 115% Analysis Date = 04/09/16 Pct Recovery = 115% Analysis Date = 03/30/16 Pct Recovery = 115% Analysis Date = 03/30/16 Pct Recovery = 115% Analysis Date = 03/20/16 Pct Recovery = 115% Analysis Date = 03/20/16 Pct Recovery = 115% Analysis Date = 03/10/16 Pct Recovery = 115% Analysis Date = 03/10/16 Pct Recovery = 115% Analysis Date = 02/29/16 Pct Recovery = 114% Analysis Date = 02/29/16 Pct Recovery = 114% Analysis Date = 02/19/16 Pct Recovery = 114% Analysis Date = 02/19/16 Pct Recovery = 114% Analysis Date = 02/09/16 Pct Recovery = 114% Analysis Date = 02/09/16 Pct Recovery = 114% Analysis Date = 01/30/16 Pct Recovery = 114% Analysis Date = 01/30/16 Pct Recovery = 114% Analysis Date = 01/20/16 Pct Recovery = 114% Analysis Date = 01/20/16 Pct Recovery = 114% Analysis Date = 01/11/16 Pct Recovery = 114% Analysis Date = 01/11/16 Pct Recovery = 114% Analysis Date = 01/01/16 Pct Recovery = 113% Analysis Date = 01/01/16 Pct Recovery = 113% Analysis Date = 12/22/15 Pct Recovery = 113% Analysis Date = 12/22/15 Pct Recovery = 113% Analysis Date = 12/12/15 Pct Recovery = 113% Analysis Date = 12/12/15 Pct Recovery = 113% Analysis Date = 12/02/15 Pct Recovery = 113% Analysis Date = 12/02/15 Pct Recovery = 113% Analysis Date = 11/22/15 Pct Recovery = 113% Analysis Date = 11/22/15 Pct Recovery = 113% Analysis Date = 11/12/15 Pct Recovery = 112% Analysis Date = 11/12/15 Pct Recovery = 112% Analysis Date = 11/02/15 Pct Recovery = 112% Analysis Date = 11/02/15 Pct Recovery = 112% Analysis Date = 10/23/15 Pct Recovery = 112% Analysis Date = 10/23/15 Pct Recovery = 112% Analysis Date = 10/13/15 Pct Recovery = 112% Analysis Date = 10/13/15 Pct Recovery = 112% Analysis Date = 10/04/15 Pct Recovery = 112% Analysis Date = 10/04/15 Pct Recovery = 112% Analysis Date = 09/24/15 Pct Recovery = 111% Analysis Date = 09/24/15 Pct Recovery = 111% Analysis Date = 09/14/15 Pct Recovery = 111% Analysis Date = 09/14/15 Pct Recovery = 111% Analysis Date = 09/04/15 Pct Recovery = 111% Analysis Date = 09/04/15 Pct Recovery = 111% Analysis Date = 08/25/15 Pct Recovery = 111% Analysis Date = 08/25/15 Pct Recovery = 111% Analysis Date = 08/15/15 Pct Recovery = 110% Analysis Date = 08/15/15 Pct Recovery = 110% Analysis Date = 08/05/15 Pct Recovery = 110% Analysis Date = 08/05/15 Pct Recovery = 110% Analysis Date = 07/26/15 Pct Recovery = 110% Analysis Date = 07/26/15 Pct Recovery = 110% Analysis Date = 07/16/15 Pct Recovery = 110% Analysis Date = 07/16/15 Pct Recovery = 110% Analysis Date = 07/06/15 Pct Recovery = 110% Analysis Date = 07/06/15 Pct Recovery = 110% Analysis Date = 06/27/15 Pct Recovery = 110% Analysis Date = 06/27/15 Pct Recovery = 110% Analysis Date = 06/17/15 Pct Recovery = 109% Analysis Date = 06/17/15 Pct Recovery = 109% Analysis Date = 06/07/15 Pct Recovery = 109% Analysis Date = 06/07/15 Pct Recovery = 109% Analysis Date = 05/28/15 Pct Recovery = 109% Analysis Date = 05/28/15 Pct Recovery = 109% Analysis Date = 05/18/15 Pct Recovery = 109% Analysis Date = 05/18/15 Pct Recovery = 109% Analysis Date = 05/08/15 Pct Recovery = 109% Analysis Date = 05/08/15 Pct Recovery = 109% Analysis Date = 04/28/15 Pct Recovery = 109% Analysis Date = 04/28/15 Pct Recovery = 109% Analysis Date = 04/18/15 Pct Recovery = 109% Analysis Date = 04/18/15 Pct Recovery = 109% Analysis Date = 04/08/15 Pct Recovery = 109% Analysis Date = 04/08/15 Pct Recovery = 109% Analysis Date = 03/29/15 Pct Recovery = 109% Analysis Date = 03/29/15 Pct Recovery = 109% Analysis Date = 03/20/15 Pct Recovery = 109% Analysis Date = 03/20/15 Pct Recovery = 109% Analysis Date = 03/10/15 Pct Recovery = 109% Analysis Date = 03/10/15 Pct Recovery = 109% Analysis Date = 02/28/15 Pct Recovery = 109% Analysis Date = 02/28/15 Pct Recovery = 109% Analysis Date = 02/18/15 Pct Recovery = 110% Analysis Date = 02/18/15 Pct Recovery = 110% Analysis Date = 02/08/15 Pct Recovery = 110% Analysis Date = 02/08/15 Pct Recovery = 110% Analysis Date = 01/29/15 Pct Recovery = 110% Analysis Date = 01/29/15 Pct Recovery = 110% Analysis Date = 01/19/15 Pct Recovery = 110% Analysis Date = 01/19/15 Pct Recovery = 110% Analysis Date = 01/09/15 Pct Recovery = 110% Analysis Date = 01/09/15 Pct Recovery = 110% Analysis Date = 12/30/14 Pct Recovery = 110% Analysis Date = 12/30/14 Pct Recovery = 110% Analysis Date = 12/20/14 Pct Recovery = 110% Analysis Date = 12/20/14 Pct Recovery = 110% Analysis Date = 12/11/14 Pct Recovery = 110% Analysis Date = 12/11/14 Pct Recovery = 110% Analysis Date = 12/01/14 Pct Recovery = 110% Analysis Date = 12/01/14 Pct Recovery = 110% Analysis Date = 11/21/14 Pct Recovery = 111% Analysis Date = 11/21/14 Pct Recovery = 111% Analysis Date = 11/11/14 Pct Recovery = 111% Analysis Date = 11/11/14 Pct Recovery = 111% Analysis Date = 11/01/14 Pct Recovery = 111% Analysis Date = 11/01/14 Pct Recovery = 111% Analysis Date = 10/22/14 Pct Recovery = 111% Analysis Date = 10/22/14 Pct Recovery = 111% Analysis Date = 10/12/14 Pct Recovery = 111% Analysis Date = 10/12/14 Pct Recovery = 111% Analysis Date = 10/02/14 Pct Recovery = 112% Analysis Date = 10/02/14 Pct Recovery = 112% Analysis Date = 09/22/14 Pct Recovery = 112% Analysis Date = 09/22/14 Pct Recovery = 112% Analysis Date = 09/12/14 Pct Recovery = 112% Analysis Date = 09/12/14 Pct Recovery = 112% Analysis Date = 09/03/14 Pct Recovery = 113% Analysis Date = 09/03/14 Pct Recovery = 113% Analysis Date = 08/24/14 Pct Recovery = 113% Analysis Date = 08/24/14 Pct Recovery = 113% Analysis Date = 08/14/14 Pct Recovery = 113% Analysis Date = 08/14/14 Pct Recovery = 113% Analysis Date = 08/04/14 Pct Recovery = 114% Analysis Date = 08/04/14 Pct Recovery = 114% Analysis Date = 07/25/14 Pct Recovery = 114% Analysis Date = 07/25/14 Pct Recovery = 114% Analysis Date = 07/15/14 Pct Recovery = 114% Analysis Date = 07/15/14 Pct Recovery = 114% Analysis Date = 07/05/14 Pct Recovery = 115% Analysis Date = 07/05/14 Pct Recovery = 115% Analysis Date = 06/25/14 Pct Recovery = 115% Analysis Date = 06/25/14 Pct Recovery = 115% Analysis Date = 06/15/14 Pct Recovery = 116% Analysis Date = 06/15/14 Pct Recovery = 116% Analysis Date = 06/05/14 Pct Recovery = 117% Analysis Date = 06/05/14 Pct Recovery = 117% Analysis Date = 05/27/14 Pct Recovery = 117% Analysis Date = 05/27/14 Pct Recovery = 117% Analysis Date = 05/17/14 Pct Recovery = 117% Analysis Date = 05/17/14 Pct Recovery = 117% Analysis Date = 05/07/14 Pct Recovery = 118% Analysis Date = 05/07/14 Pct Recovery = 118% Analysis Date = 04/27/14 Pct Recovery = 118% Analysis Date = 04/27/14 Pct Recovery = 118% Analysis Date = 04/17/14 Pct Recovery = 119% Analysis Date = 04/17/14 Pct Recovery = 119% Analysis Date = 04/07/14 Pct Recovery = 119% Analysis Date = 04/07/14 Pct Recovery = 119% Analysis Date = 03/28/14 Pct Recovery = 119% Analysis Date = 03/28/14 Pct Recovery = 119% Analysis Date = 03/18/14 Pct Recovery = 120% Analysis Date = 03/18/14 Pct Recovery = 120% Analysis Date = 03/08/14 Pct Recovery = 120% Analysis Date = 03/08/14 Pct Recovery = 120% Analysis Date = 02/26/14 Pct Recovery = 121% Analysis Date = 02/26/14 Pct Recovery = 121% Analysis Date = 02/17/14 Pct Recovery = 121% Analysis Date = 02/17/14 Pct Recovery = 121% Analysis Date = 02/07/14 Pct Recovery = 121% Analysis Date = 02/07/14 Pct Recovery = 121% Analysis Date = 01/28/14 Pct Recovery = 122% Analysis Date = 01/28/14 Pct Recovery = 122% Analysis Date = 01/18/14 Pct Recovery = 122% Analysis Date = 01/18/14 Pct Recovery = 122% Analysis Date = 01/08/14 Pct Recovery = 123% Analysis Date = 01/08/14 Pct Recovery = 123% Analysis Date = 12/29/13 Pct Recovery = 123% Analysis Date = 12/29/13 Pct Recovery = 123% Analysis Date = 12/19/13 Pct Recovery = 123% Analysis Date = 12/19/13 Pct Recovery = 123% Analysis Date = 12/09/13 Pct Recovery = 124% Analysis Date = 12/09/13 Pct Recovery = 124% Analysis Date = 11/29/13 Pct Recovery = 124% Analysis Date = 11/29/13 Pct Recovery = 124% Analysis Date = 11/19/13 Pct Recovery = 124% Analysis Date = 11/19/13 Pct Recovery = 124% Analysis Date = 11/10/13 Pct Recovery = 125% Analysis Date = 11/10/13 Pct Recovery = 125% Analysis Date = 10/31/13 Pct Recovery = 125% Analysis Date = 10/31/13 Pct Recovery = 125% Analysis Date = 10/21/13 Pct Recovery = 125% Analysis Date = 10/21/13 Pct Recovery = 125% Analysis Date = 10/11/13 Pct Recovery = 126% Analysis Date = 10/11/13 Pct Recovery = 126% Analysis Date = 10/01/13 Pct Recovery = 126% Analysis Date = 10/01/13 Pct Recovery = 126% Analysis Date = 09/21/13 Pct Recovery = 126% Analysis Date = 09/21/13 Pct Recovery = 126% Analysis Date = 09/11/13 Pct Recovery = 127% Analysis Date = 09/11/13 Pct Recovery = 127% Analysis Date = 09/01/13 Pct Recovery = 127% Analysis Date = 09/01/13 Pct Recovery = 127% Analysis Date = 08/22/13 Pct Recovery = 128% Analysis Date = 08/22/13 Pct Recovery = 128% Analysis Date = 08/12/13 Pct Recovery = 128% Analysis Date = 08/12/13 Pct Recovery = 128% Analysis Date = 08/03/13 Pct Recovery = 128% Analysis Date = 08/03/13 Pct Recovery = 128% Analysis Date = 07/24/13 Pct Recovery = 129% Analysis Date = 07/24/13 Pct Recovery = 129% Analysis Date = 07/14/13 Pct Recovery = 129% Analysis Date = 07/14/13 Pct Recovery = 129% Analysis Date = 07/04/13 Pct Recovery = 130% Analysis Date = 07/04/13 Pct Recovery = 130% Analysis Date = 06/24/13 Pct Recovery = 130% Analysis Date = 06/24/13 Pct Recovery = 130% Analysis Date = 06/14/13 Pct Recovery = 130% Analysis Date = 06/14/13 Pct Recovery = 130% Analysis Date = 06/04/13 Pct Recovery = 131% Analysis Date = 06/04/13 Pct Recovery = 131% Analysis Date = 05/25/13 Pct Recovery = 131% Analysis Date = 05/25/13 Pct Recovery = 131% Analysis Date = 05/15/13 Pct Recovery = 132% Analysis Date = 05/15/13 Pct Recovery = 132% Analysis Date = 05/05/13 Pct Recovery = 132% Analysis Date = 05/05/13 Pct Recovery = 132% Analysis Date = 04/26/13 Pct Recovery = 132% Analysis Date = 04/26/13 Pct Recovery = 132% Analysis Date = 04/16/13 Pct Recovery = 133% Analysis Date = 04/16/13 Pct Recovery = 133% Analysis Date = 04/06/13 Pct Recovery = 133% Analysis Date = 04/06/13 Pct Recovery = 133% Analysis Date = 03/27/13 Pct Recovery = 134% Analysis Date = 03/27/13 Pct Recovery = 134% Analysis Date = 03/17/13 Pct Recovery = 134% Analysis Date = 03/17/13 Pct Recovery = 134% Analysis Date = 03/07/13 Pct Recovery = 135% Analysis Date = 03/07/13 Pct Recovery = 135% Analysis Date = 02/25/13 Pct Recovery = 135% Analysis Date = 02/25/13 Pct Recovery = 135% Analysis Date = 02/15/13 Pct Recovery = 135% Analysis Date = 02/15/13 Pct Recovery = 135% Analysis Date = 02/05/13 Pct Recovery = 136% Analysis Date = 02/05/13 Pct Recovery = 136% Analysis Date = 01/26/13 Pct Recovery = 136% Analysis Date = 01/26/13 Pct Recovery = 136% Analysis Date = 01/17/13 Pct Recovery = 137% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
TEBUTHIURON

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 80 119% 37% 118% 27%
Total 80 119% 37% 118% 27%

Sample Statistics
TEBUTHIURON

Characteristic N % % Basis
Plotted 80 100% Spiked
Estimated Values 15 19% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 80 .  
False Negatives 0 0% 0 out of 80
Not Spiked 54 .  
False Positives 0 0% 0 out of 54

OBSP Determination:
TEFLUTHRIN
METHOD: 2033 , TESTIDCODE: 61606GCM39

Laboratory ID = 20132490342 Lab Value = 0.096 Expected Conc. = 0.165 Report level label = 0.014 Pct Recovery = 58% Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20130810108 Lab Value = 0.078 Expected Conc. = 0.15 Report level label = 0.014 Pct Recovery = 52% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl SpecificMix = LB92783 Laboratory ID = 20130100066 Lab Value = 0.085 Expected Conc. = 0.15 Report level label = 0.014 Pct Recovery = 56% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl SpecificMix = LB92783 Laboratory ID = 20130940097 Lab Value = 0.081 Expected Conc. = 0.1495 Report level label = 0.014 Pct Recovery = 54% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = 0507-12-04.2 Laboratory ID = 20123560092 Lab Value = 0.063 Expected Conc. = 0.1495 Report level label = 0.014 Pct Recovery = 42% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = 0507-12-04.2 Laboratory ID = 20180390003 Lab Value = 0.049 Expected Conc. = 0.093 Report level label = 0.014 Pct Recovery = 53% Analysis Date = 04/06/18 SpikeMix = Spex Organics EN170808006: 100 µl & Abs 071717Pest: 100 µl SpecificMix = 071717Pest Laboratory ID = 20172510330 Lab Value = 0.045 Expected Conc. = 0.093 Report level label = 0.014 Pct Recovery = 48% Analysis Date = 12/29/17 SpikeMix = ChemService 6537100: 100 µl & Abs 071817Pest: 100 µl SpecificMix = 6537100 Laboratory ID = 20162860079 Lab Value = 0.052 Expected Conc. = 0.09 Report level label = 0.014 Pct Recovery = 58% Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl SpecificMix = 5054800 Laboratory ID = 20161880109 Lab Value = 0.066 Expected Conc. = 0.09 Report level label = 0.014 Pct Recovery = 73% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl SpecificMix = 5054800 Laboratory ID = 20163370001 Lab Value = 0.056 Expected Conc. = 0.0876 Report level label = 0.014 Pct Recovery = 64% Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl SpecificMix = LC20138V Laboratory ID = 20152750006 Lab Value = 0.043 Expected Conc. = 0.084 Report level label = 0.014 Pct Recovery = 52% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl SpecificMix = EN150514012 Laboratory ID = 20152460215 Lab Value = 0.044 Expected Conc. = 0.084 Report level label = 0.014 Pct Recovery = 52% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl SpecificMix = EN150514012 Laboratory ID = 20132140002 Lab Value = 0.052 Expected Conc. = 0.0827 Report level label = 0.014 Pct Recovery = 62% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl SpecificMix = LB99392 Laboratory ID = 20131370001 Lab Value = 0.056 Expected Conc. = 0.0827 Report level label = 0.014 Pct Recovery = 68% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl SpecificMix = LB99392 Laboratory ID = 20140370077 Lab Value = 0.047 Expected Conc. = 0.0825 Report level label = 0.014 Pct Recovery = 57% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20132560001 Lab Value = 0.050 Expected Conc. = 0.0825 Report level label = 0.014 Pct Recovery = 61% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20171380001 Lab Value = 0.036 Expected Conc. = 0.072 Report level label = 0.014 Pct Recovery = 51% Analysis Date = 06/07/17 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 5054800 Laboratory ID = 20170960001 Lab Value = 0.037 Expected Conc. = 0.072 Report level label = 0.014 Pct Recovery = 51% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl SpecificMix = 5054800 Laboratory ID = 20161740258 Lab Value = 0.029 Expected Conc. = 0.072 Report level label = 0.014 Pct Recovery = 40% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 5054800 Laboratory ID = 20171720140 Lab Value = 0.049 Expected Conc. = 0.0701 Report level label = 0.014 Pct Recovery = 70% Analysis Date = 08/31/17 SpikeMix = Supelco LC20138V: 80 µl & Phenova B20160331: 80 µl SpecificMix = LC20138V Laboratory ID = 20170740063 Lab Value = 0.048 Expected Conc. = 0.0701 Report level label = 0.014 Pct Recovery = 68% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl SpecificMix = LC20138V Laboratory ID = 20161470001 Lab Value = 0.044 Expected Conc. = 0.0701 Report level label = 0.014 Pct Recovery = 63% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl SpecificMix = LC20138V Laboratory ID = 20130390105 Lab Value = 0.029 Expected Conc. = 0.06 Report level label = 0.014 Pct Recovery = 48% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl SpecificMix = LB92783 Laboratory ID = 20130510051 Lab Value = 0.030 Expected Conc. = 0.0598 Report level label = 0.014 Pct Recovery = 50% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl SpecificMix = 0507-12-04.2 Laboratory ID = 20150430092 Lab Value = 0.034 Expected Conc. = 0.0559 Report level label = 0.014 Pct Recovery = 61% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl SpecificMix = E1140407002 Laboratory ID = 20143110108 Lab Value = 0.029 Expected Conc. = 0.0559 Report level label = 0.014 Pct Recovery = 52% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl SpecificMix = E1140407002 Laboratory ID = 20142720002 Lab Value = 0.029 Expected Conc. = 0.0559 Report level label = 0.014 Pct Recovery = 52% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl SpecificMix = E1140407002 Laboratory ID = 20141770149 Lab Value = 0.029 Expected Conc. = 0.0559 Report level label = 0.014 Pct Recovery = 52% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl SpecificMix = E1140407002 Laboratory ID = 20143240095 Lab Value = 0.035 Expected Conc. = 0.0558 Report level label = 0.014 Pct Recovery = 63% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl SpecificMix = 032714 Laboratory ID = 20142270001 Lab Value = 0.029 Expected Conc. = 0.0558 Report level label = 0.014 Pct Recovery = 52% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl SpecificMix = 032714 Laboratory ID = 20141220025 Lab Value = 0.039 Expected Conc. = 0.0558 Report level label = 0.014 Pct Recovery = 69% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl SpecificMix = 032714 Laboratory ID = 20173480003 Lab Value = 0.026 Expected Conc. = 0.0465 Report level label = 0.014 Pct Recovery = 57% Analysis Date = 04/05/18 SpikeMix = Abs 071717Pest: 50 µl & ChemService 6567600: 50 µl SpecificMix = 071717Pest Laboratory ID = 20172370001 Lab Value = 0.028 Expected Conc. = 0.0465 Report level label = 0.014 Pct Recovery = 60% Analysis Date = 11/18/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6537100: 50 µl SpecificMix = 6537100 Laboratory ID = 20172230001 Lab Value = 0.035 Expected Conc. = 0.0465 Report level label = 0.014 Pct Recovery = 75% Analysis Date = 10/19/17 SpikeMix = ChemService 6472100: 50 µl & Abs 071717Pest: 50 µl SpecificMix = 071717Pest Laboratory ID = 20160630046 Lab Value = 0.022 Expected Conc. = 0.042 Report level label = 0.014 Pct Recovery = 51% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = EN150514012 Laboratory ID = 20153440001 Lab Value = 0.019 Expected Conc. = 0.042 Report level label = 0.014 Pct Recovery = 45% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = EN150514012 Laboratory ID = 20152330039 Lab Value = 0.024 Expected Conc. = 0.042 Report level label = 0.014 Pct Recovery = 56% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl SpecificMix = 041415 Laboratory ID = 20151900132 Lab Value = 0.027 Expected Conc. = 0.042 Report level label = 0.014 Pct Recovery = 65% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl SpecificMix = 041415 Laboratory ID = 20151270112 Lab Value = 0.031 Expected Conc. = 0.042 Report level label = 0.014 Pct Recovery = 73% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl SpecificMix = 041415 Laboratory ID = 20172020035 Lab Value = 0.025 Expected Conc. = 0.0372 Report level label = 0.014 Pct Recovery = 67% Analysis Date = 11/07/17 SpikeMix = Abs 071717Pest: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 071717Pest Laboratory ID = 20171940002 Lab Value = 0.021 Expected Conc. = 0.036 Report level label = 0.014 Pct Recovery = 57% Analysis Date = 11/10/17 SpikeMix = ChemService 5054800: 40 µl & NSI 041816: 40 µl SpecificMix = 5054800 Laboratory ID = 20170460061 Lab Value = 0.020 Expected Conc. = 0.036 Report level label = 0.014 Pct Recovery = 56% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl SpecificMix = 5054800 Laboratory ID = 20163560019 Lab Value = 0.020 Expected Conc. = 0.036 Report level label = 0.014 Pct Recovery = 57% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl SpecificMix = 5054800 Laboratory ID = 20162150213 Lab Value = 0.021 Expected Conc. = 0.036 Report level label = 0.014 Pct Recovery = 59% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl SpecificMix = 5054800 Laboratory ID = 20171510080 Lab Value = 0.022 Expected Conc. = 0.035 Report level label = 0.014 Pct Recovery = 62% Analysis Date = 06/09/17 SpikeMix = Supelco LC20138V: 40 µl & Crescent 03FF076: 40 µl SpecificMix = LC20138V Laboratory ID = 20162520001 Lab Value = 0.027 Expected Conc. = 0.035 Report level label = 0.014 Pct Recovery = 78% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl SpecificMix = LC20138V Laboratory ID = 20162660005 Lab Value = 0.019 Expected Conc. = 0.035 Report level label = 0.014 Pct Recovery = 53% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl SpecificMix = LC20138V Laboratory ID = 20162020124 Lab Value = 0.020 Expected Conc. = 0.035 Report level label = 0.014 Pct Recovery = 58% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl SpecificMix = LC20138V Laboratory ID = 20140510043 Lab Value = 0.019 Expected Conc. = 0.0331 Report level label = 0.014 Pct Recovery = 56% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl SpecificMix = LB99392 Laboratory ID = 20133470008 Lab Value = 0.019 Expected Conc. = 0.0331 Report level label = 0.014 Pct Recovery = 56% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl SpecificMix = LB99392 Laboratory ID = 20133190012 Lab Value = 0.019 Expected Conc. = 0.0331 Report level label = 0.014 Pct Recovery = 58% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = LB99392 Laboratory ID = 20133050050 Lab Value = 0.023 Expected Conc. = 0.0331 Report level label = 0.014 Pct Recovery = 69% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl SpecificMix = LB99392 Laboratory ID = 20133580036 Lab Value = 0.014 Expected Conc. = 0.033 Report level label = 0.014 Pct Recovery = 42% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20131790009 Lab Value = 0.013 Expected Conc. = 0.033 Report level label = 0.014 Pct Recovery = 41% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20131510026 Lab Value = 0.018 Expected Conc. = 0.033 Report level label = 0.014 Pct Recovery = 56% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20142470041 Lab Value = 0.017 Expected Conc. = 0.0279 Report level label = 0.014 Pct Recovery = 60% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141910243 Lab Value = 0.015 Expected Conc. = 0.0279 Report level label = 0.014 Pct Recovery = 54% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141640076 Lab Value = 0.017 Expected Conc. = 0.0279 Report level label = 0.014 Pct Recovery = 62% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = E1140407002 Laboratory ID = 20141360094 Lab Value = 0.014 Expected Conc. = 0.0279 Report level label = 0.014 Pct Recovery = 50% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = E1140407002 Laboratory ID = 20180940080 Lab Value = 0.016 Expected Conc. = 0.0279 Report level label = 0.014 Pct Recovery = 56% Analysis Date = 05/31/18 SpikeMix = ChemService 6472100: 30 µl & Abs 071717Pest: 30 µl SpecificMix = 071717Pest Laboratory ID = 20180730064 Lab Value = 0.019 Expected Conc. = 0.0279 Report level label = 0.014 Pct Recovery = 70% Analysis Date = 05/16/18 SpikeMix = Abs 071717Pest: 30 µl & Abs 071817Pest: 30 µl SpecificMix = 071717Pest Laboratory ID = 20173120093 Lab Value = 0.018 Expected Conc. = 0.0279 Report level label = 0.014 Pct Recovery = 65% Analysis Date = 03/10/18 SpikeMix = ChemService 6472100: 30 µl & ChemService 6537100: 30 µl SpecificMix = 6537100 Laboratory ID = 20172780018 Lab Value = 0.014 Expected Conc. = 0.0279 Report level label = 0.014 Pct Recovery = 51% Analysis Date = 02/08/18 SpikeMix = ChemService 6537100: 30 µl & Abs 071817Pest: 30 µl SpecificMix = 6537100 Laboratory ID = 20150150115 Lab Value = 0.016 Expected Conc. = 0.0279 Report level label = 0.014 Pct Recovery = 56% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl SpecificMix = 032714 Laboratory ID = 20142820151 Lab Value = 0.020 Expected Conc. = 0.0279 Report level label = 0.014 Pct Recovery = 72% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl SpecificMix = 032714 Laboratory ID = 20141490205 Lab Value = 0.018 Expected Conc. = 0.0279 Report level label = 0.014 Pct Recovery = 64% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = 032714 Laboratory ID = 20141080004 Lab Value = 0.016 Expected Conc. = 0.0279 Report level label = 0.014 Pct Recovery = 58% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl SpecificMix = 032714 Laboratory ID = 20161050143 Lab Value = 0.013 Expected Conc. = 0.021 Report level label = 0.014 Pct Recovery = 61% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 041415 Laboratory ID = 20160560044 Lab Value = 0.011 Expected Conc. = 0.021 Report level label = 0.014 Pct Recovery = 54% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl SpecificMix = 041415 Laboratory ID = 20160210080 Lab Value = 0.011 Expected Conc. = 0.021 Report level label = 0.014 Pct Recovery = 52% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 041415 Laboratory ID = 20160070059 Lab Value = 0.012 Expected Conc. = 0.021 Report level label = 0.014 Pct Recovery = 56% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = EN150514012 Laboratory ID = 20153160001 Lab Value = 0.012 Expected Conc. = 0.021 Report level label = 0.014 Pct Recovery = 56% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = EN150514012 Laboratory ID = 20152950078 Lab Value = 0.009 Expected Conc. = 0.021 Report level label = 0.014 Pct Recovery = 41% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 041415 Laboratory ID = 20152040177 Lab Value = 0.013 Expected Conc. = 0.021 Report level label = 0.014 Pct Recovery = 61% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl SpecificMix = 041415 Laboratory ID = 20151760208 Lab Value = 0.014 Expected Conc. = 0.021 Report level label = 0.014 Pct Recovery = 68% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl SpecificMix = EN150514012 Laboratory ID = 20151480170 Lab Value = 0.012 Expected Conc. = 0.021 Report level label = 0.014 Pct Recovery = 56% Analysis Date = 06/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150514012 Laboratory ID = 20151210037 Lab Value = 0.014 Expected Conc. = 0.021 Report level label = 0.014 Pct Recovery = 67% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 041415 Analysis Date = 05/31/18 Pct Recovery = 61% Analysis Date = 05/21/18 Pct Recovery = 61% Analysis Date = 05/21/18 Pct Recovery = 61% Analysis Date = 05/11/18 Pct Recovery = 61% Analysis Date = 05/11/18 Pct Recovery = 61% Analysis Date = 05/01/18 Pct Recovery = 61% Analysis Date = 05/01/18 Pct Recovery = 61% Analysis Date = 04/21/18 Pct Recovery = 61% Analysis Date = 04/21/18 Pct Recovery = 61% Analysis Date = 04/11/18 Pct Recovery = 61% Analysis Date = 04/11/18 Pct Recovery = 61% Analysis Date = 04/02/18 Pct Recovery = 61% Analysis Date = 04/02/18 Pct Recovery = 61% Analysis Date = 03/23/18 Pct Recovery = 61% Analysis Date = 03/23/18 Pct Recovery = 61% Analysis Date = 03/13/18 Pct Recovery = 61% Analysis Date = 03/13/18 Pct Recovery = 61% Analysis Date = 03/03/18 Pct Recovery = 61% Analysis Date = 03/03/18 Pct Recovery = 61% Analysis Date = 02/21/18 Pct Recovery = 61% Analysis Date = 02/21/18 Pct Recovery = 61% Analysis Date = 02/12/18 Pct Recovery = 61% Analysis Date = 02/12/18 Pct Recovery = 61% Analysis Date = 02/02/18 Pct Recovery = 61% Analysis Date = 02/02/18 Pct Recovery = 61% Analysis Date = 01/23/18 Pct Recovery = 61% Analysis Date = 01/23/18 Pct Recovery = 61% Analysis Date = 01/13/18 Pct Recovery = 61% Analysis Date = 01/13/18 Pct Recovery = 61% Analysis Date = 01/03/18 Pct Recovery = 60% Analysis Date = 01/03/18 Pct Recovery = 60% Analysis Date = 12/25/17 Pct Recovery = 60% Analysis Date = 12/25/17 Pct Recovery = 60% Analysis Date = 12/15/17 Pct Recovery = 60% Analysis Date = 12/15/17 Pct Recovery = 60% Analysis Date = 12/05/17 Pct Recovery = 60% Analysis Date = 12/05/17 Pct Recovery = 60% Analysis Date = 11/25/17 Pct Recovery = 60% Analysis Date = 11/25/17 Pct Recovery = 60% Analysis Date = 11/15/17 Pct Recovery = 60% Analysis Date = 11/15/17 Pct Recovery = 60% Analysis Date = 11/05/17 Pct Recovery = 60% Analysis Date = 11/05/17 Pct Recovery = 60% Analysis Date = 10/27/17 Pct Recovery = 60% Analysis Date = 10/27/17 Pct Recovery = 60% Analysis Date = 10/17/17 Pct Recovery = 60% Analysis Date = 10/17/17 Pct Recovery = 60% Analysis Date = 10/07/17 Pct Recovery = 60% Analysis Date = 10/07/17 Pct Recovery = 60% Analysis Date = 09/27/17 Pct Recovery = 60% Analysis Date = 09/27/17 Pct Recovery = 60% Analysis Date = 09/17/17 Pct Recovery = 60% Analysis Date = 09/17/17 Pct Recovery = 60% Analysis Date = 09/08/17 Pct Recovery = 60% Analysis Date = 09/08/17 Pct Recovery = 60% Analysis Date = 08/29/17 Pct Recovery = 60% Analysis Date = 08/29/17 Pct Recovery = 60% Analysis Date = 08/19/17 Pct Recovery = 60% Analysis Date = 08/19/17 Pct Recovery = 60% Analysis Date = 08/09/17 Pct Recovery = 60% Analysis Date = 08/09/17 Pct Recovery = 60% Analysis Date = 07/30/17 Pct Recovery = 60% Analysis Date = 07/30/17 Pct Recovery = 60% Analysis Date = 07/21/17 Pct Recovery = 60% Analysis Date = 07/21/17 Pct Recovery = 60% Analysis Date = 07/11/17 Pct Recovery = 59% Analysis Date = 07/11/17 Pct Recovery = 59% Analysis Date = 07/01/17 Pct Recovery = 59% Analysis Date = 07/01/17 Pct Recovery = 59% Analysis Date = 06/21/17 Pct Recovery = 59% Analysis Date = 06/21/17 Pct Recovery = 59% Analysis Date = 06/11/17 Pct Recovery = 59% Analysis Date = 06/11/17 Pct Recovery = 59% Analysis Date = 06/02/17 Pct Recovery = 59% Analysis Date = 06/02/17 Pct Recovery = 59% Analysis Date = 05/23/17 Pct Recovery = 59% Analysis Date = 05/23/17 Pct Recovery = 59% Analysis Date = 05/13/17 Pct Recovery = 59% Analysis Date = 05/13/17 Pct Recovery = 59% Analysis Date = 05/03/17 Pct Recovery = 59% Analysis Date = 05/03/17 Pct Recovery = 59% Analysis Date = 04/23/17 Pct Recovery = 59% Analysis Date = 04/23/17 Pct Recovery = 59% Analysis Date = 04/13/17 Pct Recovery = 59% Analysis Date = 04/13/17 Pct Recovery = 59% Analysis Date = 04/04/17 Pct Recovery = 59% Analysis Date = 04/04/17 Pct Recovery = 59% Analysis Date = 03/25/17 Pct Recovery = 59% Analysis Date = 03/25/17 Pct Recovery = 59% Analysis Date = 03/15/17 Pct Recovery = 59% Analysis Date = 03/15/17 Pct Recovery = 59% Analysis Date = 03/05/17 Pct Recovery = 59% Analysis Date = 03/05/17 Pct Recovery = 59% Analysis Date = 02/23/17 Pct Recovery = 59% Analysis Date = 02/23/17 Pct Recovery = 59% Analysis Date = 02/14/17 Pct Recovery = 59% Analysis Date = 02/14/17 Pct Recovery = 59% Analysis Date = 02/04/17 Pct Recovery = 59% Analysis Date = 02/04/17 Pct Recovery = 59% Analysis Date = 01/25/17 Pct Recovery = 59% Analysis Date = 01/25/17 Pct Recovery = 59% Analysis Date = 01/15/17 Pct Recovery = 58% Analysis Date = 01/15/17 Pct Recovery = 58% Analysis Date = 01/05/17 Pct Recovery = 58% Analysis Date = 01/05/17 Pct Recovery = 58% Analysis Date = 12/27/16 Pct Recovery = 58% Analysis Date = 12/27/16 Pct Recovery = 58% Analysis Date = 12/17/16 Pct Recovery = 58% Analysis Date = 12/17/16 Pct Recovery = 58% Analysis Date = 12/07/16 Pct Recovery = 58% Analysis Date = 12/07/16 Pct Recovery = 58% Analysis Date = 11/27/16 Pct Recovery = 58% Analysis Date = 11/27/16 Pct Recovery = 58% Analysis Date = 11/17/16 Pct Recovery = 58% Analysis Date = 11/17/16 Pct Recovery = 58% Analysis Date = 11/08/16 Pct Recovery = 58% Analysis Date = 11/08/16 Pct Recovery = 58% Analysis Date = 10/29/16 Pct Recovery = 58% Analysis Date = 10/29/16 Pct Recovery = 58% Analysis Date = 10/19/16 Pct Recovery = 58% Analysis Date = 10/19/16 Pct Recovery = 58% Analysis Date = 10/09/16 Pct Recovery = 58% Analysis Date = 10/09/16 Pct Recovery = 58% Analysis Date = 09/29/16 Pct Recovery = 58% Analysis Date = 09/29/16 Pct Recovery = 58% Analysis Date = 09/19/16 Pct Recovery = 58% Analysis Date = 09/19/16 Pct Recovery = 58% Analysis Date = 09/10/16 Pct Recovery = 58% Analysis Date = 09/10/16 Pct Recovery = 58% Analysis Date = 08/31/16 Pct Recovery = 58% Analysis Date = 08/31/16 Pct Recovery = 58% Analysis Date = 08/21/16 Pct Recovery = 58% Analysis Date = 08/21/16 Pct Recovery = 58% Analysis Date = 08/11/16 Pct Recovery = 58% Analysis Date = 08/11/16 Pct Recovery = 58% Analysis Date = 08/01/16 Pct Recovery = 58% Analysis Date = 08/01/16 Pct Recovery = 58% Analysis Date = 07/23/16 Pct Recovery = 58% Analysis Date = 07/23/16 Pct Recovery = 58% Analysis Date = 07/13/16 Pct Recovery = 58% Analysis Date = 07/13/16 Pct Recovery = 58% Analysis Date = 07/03/16 Pct Recovery = 58% Analysis Date = 07/03/16 Pct Recovery = 58% Analysis Date = 06/23/16 Pct Recovery = 58% Analysis Date = 06/23/16 Pct Recovery = 58% Analysis Date = 06/13/16 Pct Recovery = 58% Analysis Date = 06/13/16 Pct Recovery = 58% Analysis Date = 06/04/16 Pct Recovery = 58% Analysis Date = 06/04/16 Pct Recovery = 58% Analysis Date = 05/25/16 Pct Recovery = 58% Analysis Date = 05/25/16 Pct Recovery = 58% Analysis Date = 05/15/16 Pct Recovery = 58% Analysis Date = 05/15/16 Pct Recovery = 58% Analysis Date = 05/05/16 Pct Recovery = 58% Analysis Date = 05/05/16 Pct Recovery = 58% Analysis Date = 04/25/16 Pct Recovery = 58% Analysis Date = 04/25/16 Pct Recovery = 58% Analysis Date = 04/16/16 Pct Recovery = 57% Analysis Date = 04/16/16 Pct Recovery = 57% Analysis Date = 04/06/16 Pct Recovery = 57% Analysis Date = 04/06/16 Pct Recovery = 57% Analysis Date = 03/27/16 Pct Recovery = 57% Analysis Date = 03/27/16 Pct Recovery = 57% Analysis Date = 03/17/16 Pct Recovery = 57% Analysis Date = 03/17/16 Pct Recovery = 57% Analysis Date = 03/07/16 Pct Recovery = 57% Analysis Date = 03/07/16 Pct Recovery = 57% Analysis Date = 02/26/16 Pct Recovery = 57% Analysis Date = 02/26/16 Pct Recovery = 57% Analysis Date = 02/17/16 Pct Recovery = 57% Analysis Date = 02/17/16 Pct Recovery = 57% Analysis Date = 02/07/16 Pct Recovery = 57% Analysis Date = 02/07/16 Pct Recovery = 57% Analysis Date = 01/28/16 Pct Recovery = 57% Analysis Date = 01/28/16 Pct Recovery = 57% Analysis Date = 01/18/16 Pct Recovery = 57% Analysis Date = 01/18/16 Pct Recovery = 57% Analysis Date = 01/08/16 Pct Recovery = 57% Analysis Date = 01/08/16 Pct Recovery = 57% Analysis Date = 12/30/15 Pct Recovery = 57% Analysis Date = 12/30/15 Pct Recovery = 57% Analysis Date = 12/20/15 Pct Recovery = 57% Analysis Date = 12/20/15 Pct Recovery = 57% Analysis Date = 12/10/15 Pct Recovery = 57% Analysis Date = 12/10/15 Pct Recovery = 57% Analysis Date = 11/30/15 Pct Recovery = 57% Analysis Date = 11/30/15 Pct Recovery = 57% Analysis Date = 11/20/15 Pct Recovery = 57% Analysis Date = 11/20/15 Pct Recovery = 57% Analysis Date = 11/11/15 Pct Recovery = 57% Analysis Date = 11/11/15 Pct Recovery = 57% Analysis Date = 11/01/15 Pct Recovery = 57% Analysis Date = 11/01/15 Pct Recovery = 57% Analysis Date = 10/22/15 Pct Recovery = 57% Analysis Date = 10/22/15 Pct Recovery = 57% Analysis Date = 10/12/15 Pct Recovery = 57% Analysis Date = 10/12/15 Pct Recovery = 57% Analysis Date = 10/02/15 Pct Recovery = 57% Analysis Date = 10/02/15 Pct Recovery = 57% Analysis Date = 09/23/15 Pct Recovery = 57% Analysis Date = 09/23/15 Pct Recovery = 57% Analysis Date = 09/13/15 Pct Recovery = 57% Analysis Date = 09/13/15 Pct Recovery = 57% Analysis Date = 09/03/15 Pct Recovery = 57% Analysis Date = 09/03/15 Pct Recovery = 57% Analysis Date = 08/24/15 Pct Recovery = 57% Analysis Date = 08/24/15 Pct Recovery = 57% Analysis Date = 08/14/15 Pct Recovery = 57% Analysis Date = 08/14/15 Pct Recovery = 57% Analysis Date = 08/04/15 Pct Recovery = 57% Analysis Date = 08/04/15 Pct Recovery = 57% Analysis Date = 07/26/15 Pct Recovery = 58% Analysis Date = 07/26/15 Pct Recovery = 58% Analysis Date = 07/16/15 Pct Recovery = 58% Analysis Date = 07/16/15 Pct Recovery = 58% Analysis Date = 07/06/15 Pct Recovery = 58% Analysis Date = 07/06/15 Pct Recovery = 58% Analysis Date = 06/26/15 Pct Recovery = 58% Analysis Date = 06/26/15 Pct Recovery = 58% Analysis Date = 06/16/15 Pct Recovery = 58% Analysis Date = 06/16/15 Pct Recovery = 58% Analysis Date = 06/07/15 Pct Recovery = 58% Analysis Date = 06/07/15 Pct Recovery = 58% Analysis Date = 05/28/15 Pct Recovery = 58% Analysis Date = 05/28/15 Pct Recovery = 58% Analysis Date = 05/18/15 Pct Recovery = 58% Analysis Date = 05/18/15 Pct Recovery = 58% Analysis Date = 05/08/15 Pct Recovery = 58% Analysis Date = 05/08/15 Pct Recovery = 58% Analysis Date = 04/28/15 Pct Recovery = 58% Analysis Date = 04/28/15 Pct Recovery = 58% Analysis Date = 04/19/15 Pct Recovery = 58% Analysis Date = 04/19/15 Pct Recovery = 58% Analysis Date = 04/09/15 Pct Recovery = 58% Analysis Date = 04/09/15 Pct Recovery = 58% Analysis Date = 03/30/15 Pct Recovery = 58% Analysis Date = 03/30/15 Pct Recovery = 58% Analysis Date = 03/20/15 Pct Recovery = 58% Analysis Date = 03/20/15 Pct Recovery = 58% Analysis Date = 03/10/15 Pct Recovery = 58% Analysis Date = 03/10/15 Pct Recovery = 58% Analysis Date = 02/28/15 Pct Recovery = 58% Analysis Date = 02/28/15 Pct Recovery = 58% Analysis Date = 02/19/15 Pct Recovery = 58% Analysis Date = 02/19/15 Pct Recovery = 58% Analysis Date = 02/09/15 Pct Recovery = 58% Analysis Date = 02/09/15 Pct Recovery = 58% Analysis Date = 01/30/15 Pct Recovery = 58% Analysis Date = 01/30/15 Pct Recovery = 58% Analysis Date = 01/20/15 Pct Recovery = 58% Analysis Date = 01/20/15 Pct Recovery = 58% Analysis Date = 01/10/15 Pct Recovery = 59% Analysis Date = 01/10/15 Pct Recovery = 59% Analysis Date = 01/01/15 Pct Recovery = 59% Analysis Date = 01/01/15 Pct Recovery = 59% Analysis Date = 12/22/14 Pct Recovery = 59% Analysis Date = 12/22/14 Pct Recovery = 59% Analysis Date = 12/12/14 Pct Recovery = 59% Analysis Date = 12/12/14 Pct Recovery = 59% Analysis Date = 12/02/14 Pct Recovery = 59% Analysis Date = 12/02/14 Pct Recovery = 59% Analysis Date = 11/22/14 Pct Recovery = 59% Analysis Date = 11/22/14 Pct Recovery = 59% Analysis Date = 11/13/14 Pct Recovery = 59% Analysis Date = 11/13/14 Pct Recovery = 59% Analysis Date = 11/03/14 Pct Recovery = 59% Analysis Date = 11/03/14 Pct Recovery = 59% Analysis Date = 10/24/14 Pct Recovery = 59% Analysis Date = 10/24/14 Pct Recovery = 59% Analysis Date = 10/14/14 Pct Recovery = 59% Analysis Date = 10/14/14 Pct Recovery = 59% Analysis Date = 10/04/14 Pct Recovery = 59% Analysis Date = 10/04/14 Pct Recovery = 59% Analysis Date = 09/25/14 Pct Recovery = 59% Analysis Date = 09/25/14 Pct Recovery = 59% Analysis Date = 09/15/14 Pct Recovery = 59% Analysis Date = 09/15/14 Pct Recovery = 59% Analysis Date = 09/05/14 Pct Recovery = 59% Analysis Date = 09/05/14 Pct Recovery = 59% Analysis Date = 08/26/14 Pct Recovery = 59% Analysis Date = 08/26/14 Pct Recovery = 59% Analysis Date = 08/16/14 Pct Recovery = 59% Analysis Date = 08/16/14 Pct Recovery = 59% Analysis Date = 08/06/14 Pct Recovery = 59% Analysis Date = 08/06/14 Pct Recovery = 59% Analysis Date = 07/28/14 Pct Recovery = 59% Analysis Date = 07/28/14 Pct Recovery = 59% Analysis Date = 07/18/14 Pct Recovery = 59% Analysis Date = 07/18/14 Pct Recovery = 59% Analysis Date = 07/08/14 Pct Recovery = 59% Analysis Date = 07/08/14 Pct Recovery = 59% Analysis Date = 06/28/14 Pct Recovery = 59% Analysis Date = 06/28/14 Pct Recovery = 59% Analysis Date = 06/18/14 Pct Recovery = 58% Analysis Date = 06/18/14 Pct Recovery = 58% Analysis Date = 06/09/14 Pct Recovery = 58% Analysis Date = 06/09/14 Pct Recovery = 58% Analysis Date = 05/30/14 Pct Recovery = 58% Analysis Date = 05/30/14 Pct Recovery = 58% Analysis Date = 05/20/14 Pct Recovery = 58% Analysis Date = 05/20/14 Pct Recovery = 58% Analysis Date = 05/10/14 Pct Recovery = 58% Analysis Date = 05/10/14 Pct Recovery = 58% Analysis Date = 04/30/14 Pct Recovery = 58% Analysis Date = 04/30/14 Pct Recovery = 58% Analysis Date = 04/21/14 Pct Recovery = 58% Analysis Date = 04/21/14 Pct Recovery = 58% Analysis Date = 04/11/14 Pct Recovery = 58% Analysis Date = 04/11/14 Pct Recovery = 58% Analysis Date = 04/01/14 Pct Recovery = 58% Analysis Date = 04/01/14 Pct Recovery = 58% Analysis Date = 03/22/14 Pct Recovery = 57% Analysis Date = 03/22/14 Pct Recovery = 57% Analysis Date = 03/12/14 Pct Recovery = 57% Analysis Date = 03/12/14 Pct Recovery = 57% Analysis Date = 03/03/14 Pct Recovery = 57% Analysis Date = 03/03/14 Pct Recovery = 57% Analysis Date = 02/21/14 Pct Recovery = 57% Analysis Date = 02/21/14 Pct Recovery = 57% Analysis Date = 02/11/14 Pct Recovery = 57% Analysis Date = 02/11/14 Pct Recovery = 57% Analysis Date = 02/01/14 Pct Recovery = 57% Analysis Date = 02/01/14 Pct Recovery = 57% Analysis Date = 01/22/14 Pct Recovery = 57% Analysis Date = 01/22/14 Pct Recovery = 57% Analysis Date = 01/12/14 Pct Recovery = 57% Analysis Date = 01/12/14 Pct Recovery = 57% Analysis Date = 01/03/14 Pct Recovery = 57% Analysis Date = 01/03/14 Pct Recovery = 57% Analysis Date = 12/24/13 Pct Recovery = 56% Analysis Date = 12/24/13 Pct Recovery = 56% Analysis Date = 12/14/13 Pct Recovery = 56% Analysis Date = 12/14/13 Pct Recovery = 56% Analysis Date = 12/04/13 Pct Recovery = 56% Analysis Date = 12/04/13 Pct Recovery = 56% Analysis Date = 11/24/13 Pct Recovery = 56% Analysis Date = 11/24/13 Pct Recovery = 56% Analysis Date = 11/15/13 Pct Recovery = 56% Analysis Date = 11/15/13 Pct Recovery = 56% Analysis Date = 11/05/13 Pct Recovery = 56% Analysis Date = 11/05/13 Pct Recovery = 56% Analysis Date = 10/26/13 Pct Recovery = 56% Analysis Date = 10/26/13 Pct Recovery = 56% Analysis Date = 10/16/13 Pct Recovery = 56% Analysis Date = 10/16/13 Pct Recovery = 56% Analysis Date = 10/06/13 Pct Recovery = 55% Analysis Date = 10/06/13 Pct Recovery = 55% Analysis Date = 09/27/13 Pct Recovery = 55% Analysis Date = 09/27/13 Pct Recovery = 55% Analysis Date = 09/17/13 Pct Recovery = 55% Analysis Date = 09/17/13 Pct Recovery = 55% Analysis Date = 09/07/13 Pct Recovery = 55% Analysis Date = 09/07/13 Pct Recovery = 55% Analysis Date = 08/28/13 Pct Recovery = 55% Analysis Date = 08/28/13 Pct Recovery = 55% Analysis Date = 08/18/13 Pct Recovery = 55% Analysis Date = 08/18/13 Pct Recovery = 55% Analysis Date = 08/09/13 Pct Recovery = 55% Analysis Date = 08/09/13 Pct Recovery = 55% Analysis Date = 07/30/13 Pct Recovery = 55% Analysis Date = 07/30/13 Pct Recovery = 55% Analysis Date = 07/20/13 Pct Recovery = 55% Analysis Date = 07/20/13 Pct Recovery = 55% Analysis Date = 07/10/13 Pct Recovery = 54% Analysis Date = 07/10/13 Pct Recovery = 54% Analysis Date = 06/30/13 Pct Recovery = 54% Analysis Date = 06/30/13 Pct Recovery = 54% Analysis Date = 06/20/13 Pct Recovery = 54% Analysis Date = 06/20/13 Pct Recovery = 54% Analysis Date = 06/11/13 Pct Recovery = 54% Analysis Date = 06/11/13 Pct Recovery = 54% Analysis Date = 06/01/13 Pct Recovery = 54% Analysis Date = 06/01/13 Pct Recovery = 54% Analysis Date = 05/22/13 Pct Recovery = 54% Analysis Date = 05/22/13 Pct Recovery = 54% Analysis Date = 05/12/13 Pct Recovery = 54% Analysis Date = 05/12/13 Pct Recovery = 54% Analysis Date = 05/02/13 Pct Recovery = 54% Analysis Date = 05/02/13 Pct Recovery = 54% Analysis Date = 04/23/13 Pct Recovery = 53% Analysis Date = 04/23/13 Pct Recovery = 53% Analysis Date = 04/13/13 Pct Recovery = 53% Analysis Date = 04/13/13 Pct Recovery = 53% Analysis Date = 04/03/13 Pct Recovery = 53% Analysis Date = 04/03/13 Pct Recovery = 53% Analysis Date = 03/24/13 Pct Recovery = 53% Analysis Date = 03/24/13 Pct Recovery = 53% Analysis Date = 03/14/13 Pct Recovery = 53% Analysis Date = 03/14/13 Pct Recovery = 53% Analysis Date = 03/05/13 Pct Recovery = 53% Analysis Date = 03/05/13 Pct Recovery = 53% Analysis Date = 02/23/13 Pct Recovery = 53% Analysis Date = 02/23/13 Pct Recovery = 53% Analysis Date = 02/13/13 Pct Recovery = 53% Analysis Date = 02/13/13 Pct Recovery = 53% Analysis Date = 02/03/13 Pct Recovery = 53% Analysis Date = 02/03/13 Pct Recovery = 53% Analysis Date = 01/24/13 Pct Recovery = 52% Analysis Date = 01/24/13 Pct Recovery = 52% Analysis Date = 01/15/13 Pct Recovery = 52% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
TEFLUTHRIN

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 77 58% 8% 57% 8%
Total 77 58% 8% 57% 8%

Sample Statistics
TEFLUTHRIN

Characteristic N % % Basis
Plotted 77 100% Spiked
Estimated Values 77 100% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 77 .  
False Negatives 0 0% 0 out of 77
Not Spiked 57 .  
False Positives 0 0% 0 out of 57

OBSP Determination:
TERBUFOS
METHOD: 2033 , TESTIDCODE: 82675GCM35

Laboratory ID = 20130250061 Lab Value = 0.171 Expected Conc. = 0.299 Report level label = 0.018 Pct Recovery = 57% Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl SpecificMix = 05BB029 Laboratory ID = 20140100085 Lab Value = 0.202 Expected Conc. = 0.226 Report level label = 0.018 Pct Recovery = 89% Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl SpecificMix = 042413 Laboratory ID = 20130940097 Lab Value = 0.038 Expected Conc. = 0.1515 Report level label = 0.018 Pct Recovery = 25% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = 052412 Laboratory ID = 20130100066 Lab Value = 0.086 Expected Conc. = 0.1515 Report level label = 0.018 Pct Recovery = 57% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl SpecificMix = 052412 Laboratory ID = 20140230082 Lab Value = 0.109 Expected Conc. = 0.151 Report level label = 0.018 Pct Recovery = 72% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl SpecificMix = 012513 Laboratory ID = 20132420001 Lab Value = 0.097 Expected Conc. = 0.151 Report level label = 0.018 Pct Recovery = 64% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl SpecificMix = 012513 Laboratory ID = 20172510330 Lab Value = 0.091 Expected Conc. = 0.119 Report level label = 0.018 Pct Recovery = 76% Analysis Date = 12/29/17 SpikeMix = ChemService 6537100: 100 µl & Abs 071817Pest: 100 µl SpecificMix = 071817Pest Laboratory ID = 20132690010 Lab Value = 0.111 Expected Conc. = 0.113 Report level label = 0.018 Pct Recovery = 98% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl SpecificMix = 042413 Laboratory ID = 20132560001 Lab Value = 0.074 Expected Conc. = 0.113 Report level label = 0.018 Pct Recovery = 65% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl SpecificMix = 042413 Laboratory ID = 20163370001 Lab Value = 0.082 Expected Conc. = 0.112 Report level label = 0.018 Pct Recovery = 73% Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl SpecificMix = B20160331 Laboratory ID = 20163150006 Lab Value = 0.092 Expected Conc. = 0.112 Report level label = 0.018 Pct Recovery = 82% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl SpecificMix = B20160331 Laboratory ID = 20132140002 Lab Value = 0.028 Expected Conc. = 0.111 Report level label = 0.018 Pct Recovery = 25% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl SpecificMix = 04CC101 Laboratory ID = 20171720140 Lab Value = 0.091 Expected Conc. = 0.0896 Report level label = 0.018 Pct Recovery = 101% Analysis Date = 08/31/17 SpikeMix = Supelco LC20138V: 80 µl & Phenova B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20171660002 Lab Value = 0.093 Expected Conc. = 0.0896 Report level label = 0.018 Pct Recovery = 104% Analysis Date = 08/23/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20170190026 Lab Value = 0.074 Expected Conc. = 0.0896 Report level label = 0.018 Pct Recovery = 82% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20161470001 Lab Value = 0.067 Expected Conc. = 0.0896 Report level label = 0.018 Pct Recovery = 74% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20161880109 Lab Value = 0.068 Expected Conc. = 0.075 Report level label = 0.018 Pct Recovery = 90% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl SpecificMix = 03FF076 Laboratory ID = 20150720069 Lab Value = 0.041 Expected Conc. = 0.0726 Report level label = 0.018 Pct Recovery = 57% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 0227-14-08 Laboratory ID = 20141770149 Lab Value = 0.046 Expected Conc. = 0.0726 Report level label = 0.018 Pct Recovery = 64% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl SpecificMix = 0227-14-08 Laboratory ID = 20141570088 Lab Value = 0.057 Expected Conc. = 0.0726 Report level label = 0.018 Pct Recovery = 78% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl SpecificMix = 0227-14-08 Laboratory ID = 20150430092 Lab Value = 0.047 Expected Conc. = 0.072 Report level label = 0.018 Pct Recovery = 65% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl SpecificMix = 042814 Laboratory ID = 20143240095 Lab Value = 0.045 Expected Conc. = 0.072 Report level label = 0.018 Pct Recovery = 63% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl SpecificMix = 042814 Laboratory ID = 20142960086 Lab Value = 0.035 Expected Conc. = 0.072 Report level label = 0.018 Pct Recovery = 49% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 042814 Laboratory ID = 20142530087 Lab Value = 0.036 Expected Conc. = 0.072 Report level label = 0.018 Pct Recovery = 50% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl SpecificMix = 042814 Laboratory ID = 20133400002 Lab Value = 0.049 Expected Conc. = 0.0606 Report level label = 0.018 Pct Recovery = 81% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = 052412 Laboratory ID = 20132910008 Lab Value = 0.041 Expected Conc. = 0.0606 Report level label = 0.018 Pct Recovery = 67% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = 052412 Laboratory ID = 20130650005 Lab Value = 0.025 Expected Conc. = 0.0606 Report level label = 0.018 Pct Recovery = 42% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl SpecificMix = 052412 Laboratory ID = 20140860102 Lab Value = 0.034 Expected Conc. = 0.0604 Report level label = 0.018 Pct Recovery = 55% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 012513 Laboratory ID = 20131920149 Lab Value = 0.033 Expected Conc. = 0.0604 Report level label = 0.018 Pct Recovery = 55% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl SpecificMix = 012513 Laboratory ID = 20173480003 Lab Value = 0.049 Expected Conc. = 0.06 Report level label = 0.018 Pct Recovery = 82% Analysis Date = 04/05/18 SpikeMix = Abs 071717Pest: 50 µl & ChemService 6567600: 50 µl SpecificMix = 6567600 Laboratory ID = 20172560101 Lab Value = 0.033 Expected Conc. = 0.06 Report level label = 0.018 Pct Recovery = 56% Analysis Date = 12/22/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6567600: 50 µl SpecificMix = 6567600 Laboratory ID = 20170960001 Lab Value = 0.041 Expected Conc. = 0.06 Report level label = 0.018 Pct Recovery = 68% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl SpecificMix = 03FF076 Laboratory ID = 20130510051 Lab Value = 0.015 Expected Conc. = 0.0598 Report level label = 0.018 Pct Recovery = 25% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl SpecificMix = 05BB029 Laboratory ID = 20181430122 Lab Value = 0.045 Expected Conc. = 0.0595 Report level label = 0.018 Pct Recovery = 76% Analysis Date = 06/20/18 SpikeMix = Abs 071817Pest: 50 µl & Spex Organics EN170808006: 50 µl SpecificMix = 071817Pest Laboratory ID = 20161260151 Lab Value = 0.034 Expected Conc. = 0.056 Report level label = 0.018 Pct Recovery = 60% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = 3851600 Laboratory ID = 20151270112 Lab Value = 0.033 Expected Conc. = 0.056 Report level label = 0.018 Pct Recovery = 59% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl SpecificMix = 3851600 Laboratory ID = 20160770090 Lab Value = 0.031 Expected Conc. = 0.0544 Report level label = 0.018 Pct Recovery = 57% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20160630046 Lab Value = 0.026 Expected Conc. = 0.0544 Report level label = 0.018 Pct Recovery = 49% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20153510109 Lab Value = 0.026 Expected Conc. = 0.0544 Report level label = 0.018 Pct Recovery = 49% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20153440001 Lab Value = 0.024 Expected Conc. = 0.0544 Report level label = 0.018 Pct Recovery = 45% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl SpecificMix = 0406-15-01 Laboratory ID = 20133580036 Lab Value = 0.020 Expected Conc. = 0.0452 Report level label = 0.018 Pct Recovery = 44% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 042413 Laboratory ID = 20133190012 Lab Value = 0.033 Expected Conc. = 0.0452 Report level label = 0.018 Pct Recovery = 73% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 042413 Laboratory ID = 20131650073 Lab Value = 0.012 Expected Conc. = 0.0452 Report level label = 0.018 Pct Recovery = 27% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl SpecificMix = 042413 Laboratory ID = 20171160110 Lab Value = 0.042 Expected Conc. = 0.0448 Report level label = 0.018 Pct Recovery = 93% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = B20160331 Laboratory ID = 20162380004 Lab Value = 0.036 Expected Conc. = 0.0448 Report level label = 0.018 Pct Recovery = 79% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = B20160331 Laboratory ID = 20162150213 Lab Value = 0.032 Expected Conc. = 0.0448 Report level label = 0.018 Pct Recovery = 72% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl SpecificMix = B20160331 Laboratory ID = 20140730138 Lab Value = 0.027 Expected Conc. = 0.0444 Report level label = 0.018 Pct Recovery = 60% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 04CC101 Laboratory ID = 20140510043 Lab Value = 0.024 Expected Conc. = 0.0444 Report level label = 0.018 Pct Recovery = 54% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 04CC101 Laboratory ID = 20133310030 Lab Value = 0.031 Expected Conc. = 0.0444 Report level label = 0.018 Pct Recovery = 70% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl SpecificMix = 04CC101 Laboratory ID = 20132280016 Lab Value = 0.026 Expected Conc. = 0.0444 Report level label = 0.018 Pct Recovery = 58% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl SpecificMix = 04CC101 Laboratory ID = 20141840097 Lab Value = 0.019 Expected Conc. = 0.0363 Report level label = 0.018 Pct Recovery = 51% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20141490205 Lab Value = 0.029 Expected Conc. = 0.0363 Report level label = 0.018 Pct Recovery = 79% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20141420140 Lab Value = 0.022 Expected Conc. = 0.0363 Report level label = 0.018 Pct Recovery = 60% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20141360094 Lab Value = 0.019 Expected Conc. = 0.0363 Report level label = 0.018 Pct Recovery = 53% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20143370094 Lab Value = 0.012 Expected Conc. = 0.036 Report level label = 0.018 Pct Recovery = 33% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl SpecificMix = 042814 Laboratory ID = 20142820151 Lab Value = 0.015 Expected Conc. = 0.036 Report level label = 0.018 Pct Recovery = 43% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl SpecificMix = 042814 Laboratory ID = 20142470041 Lab Value = 0.013 Expected Conc. = 0.036 Report level label = 0.018 Pct Recovery = 35% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl SpecificMix = 042814 Laboratory ID = 20142200164 Lab Value = 0.013 Expected Conc. = 0.036 Report level label = 0.018 Pct Recovery = 36% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 042814 Laboratory ID = 20180730064 Lab Value = 0.028 Expected Conc. = 0.0357 Report level label = 0.018 Pct Recovery = 77% Analysis Date = 05/16/18 SpikeMix = Abs 071717Pest: 30 µl & Abs 071817Pest: 30 µl SpecificMix = 071817Pest Laboratory ID = 20180050004 Lab Value = 0.028 Expected Conc. = 0.0357 Report level label = 0.018 Pct Recovery = 77% Analysis Date = 04/05/18 SpikeMix = Abs 071817Pest: 30 µl & ChemService 6472100: 30 µl SpecificMix = 071817Pest Laboratory ID = 20172780018 Lab Value = 0.021 Expected Conc. = 0.0357 Report level label = 0.018 Pct Recovery = 59% Analysis Date = 02/08/18 SpikeMix = ChemService 6537100: 30 µl & Abs 071817Pest: 30 µl SpecificMix = 071817Pest Laboratory ID = 20172020035 Lab Value = 0.027 Expected Conc. = 0.03 Report level label = 0.018 Pct Recovery = 91% Analysis Date = 11/07/17 SpikeMix = Abs 071717Pest: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20171510080 Lab Value = 0.025 Expected Conc. = 0.03 Report level label = 0.018 Pct Recovery = 83% Analysis Date = 06/09/17 SpikeMix = Supelco LC20138V: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20170460061 Lab Value = 0.019 Expected Conc. = 0.03 Report level label = 0.018 Pct Recovery = 63% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl SpecificMix = 03FF076 Laboratory ID = 20162660005 Lab Value = 0.017 Expected Conc. = 0.03 Report level label = 0.018 Pct Recovery = 57% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl SpecificMix = 03FF076 Laboratory ID = 20161600087 Lab Value = 0.026 Expected Conc. = 0.03 Report level label = 0.018 Pct Recovery = 85% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20161340228 Lab Value = 0.017 Expected Conc. = 0.03 Report level label = 0.018 Pct Recovery = 58% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl SpecificMix = 03FF076 Laboratory ID = 20161190075 Lab Value = 0.017 Expected Conc. = 0.03 Report level label = 0.018 Pct Recovery = 56% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20160430111 Lab Value = 0.017 Expected Conc. = 0.028 Report level label = 0.018 Pct Recovery = 61% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 3851600 Laboratory ID = 20160210080 Lab Value = 0.014 Expected Conc. = 0.028 Report level label = 0.018 Pct Recovery = 51% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 3851600 Laboratory ID = 20152950078 Lab Value = 0.013 Expected Conc. = 0.028 Report level label = 0.018 Pct Recovery = 46% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl SpecificMix = 3851600 Laboratory ID = 20153030068 Lab Value = 0.021 Expected Conc. = 0.028 Report level label = 0.018 Pct Recovery = 75% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = 3851600 Laboratory ID = 20151380009 Lab Value = 0.012 Expected Conc. = 0.028 Report level label = 0.018 Pct Recovery = 42% Analysis Date = 05/30/15 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 3851600 Analysis Date = 06/20/18 Pct Recovery = 84% Analysis Date = 06/10/18 Pct Recovery = 84% Analysis Date = 06/10/18 Pct Recovery = 84% Analysis Date = 05/31/18 Pct Recovery = 83% Analysis Date = 05/31/18 Pct Recovery = 83% Analysis Date = 05/21/18 Pct Recovery = 83% Analysis Date = 05/21/18 Pct Recovery = 83% Analysis Date = 05/11/18 Pct Recovery = 83% Analysis Date = 05/11/18 Pct Recovery = 83% Analysis Date = 05/01/18 Pct Recovery = 83% Analysis Date = 05/01/18 Pct Recovery = 83% Analysis Date = 04/21/18 Pct Recovery = 83% Analysis Date = 04/21/18 Pct Recovery = 83% Analysis Date = 04/11/18 Pct Recovery = 82% Analysis Date = 04/11/18 Pct Recovery = 82% Analysis Date = 04/01/18 Pct Recovery = 82% Analysis Date = 04/01/18 Pct Recovery = 82% Analysis Date = 03/22/18 Pct Recovery = 82% Analysis Date = 03/22/18 Pct Recovery = 82% Analysis Date = 03/13/18 Pct Recovery = 82% Analysis Date = 03/13/18 Pct Recovery = 82% Analysis Date = 03/03/18 Pct Recovery = 82% Analysis Date = 03/03/18 Pct Recovery = 82% Analysis Date = 02/21/18 Pct Recovery = 81% Analysis Date = 02/21/18 Pct Recovery = 81% Analysis Date = 02/11/18 Pct Recovery = 81% Analysis Date = 02/11/18 Pct Recovery = 81% Analysis Date = 02/01/18 Pct Recovery = 81% Analysis Date = 02/01/18 Pct Recovery = 81% Analysis Date = 01/22/18 Pct Recovery = 81% Analysis Date = 01/22/18 Pct Recovery = 81% Analysis Date = 01/12/18 Pct Recovery = 80% Analysis Date = 01/12/18 Pct Recovery = 80% Analysis Date = 01/02/18 Pct Recovery = 80% Analysis Date = 01/02/18 Pct Recovery = 80% Analysis Date = 12/23/17 Pct Recovery = 80% Analysis Date = 12/23/17 Pct Recovery = 80% Analysis Date = 12/13/17 Pct Recovery = 80% Analysis Date = 12/13/17 Pct Recovery = 80% Analysis Date = 12/04/17 Pct Recovery = 79% Analysis Date = 12/04/17 Pct Recovery = 79% Analysis Date = 11/24/17 Pct Recovery = 79% Analysis Date = 11/24/17 Pct Recovery = 79% Analysis Date = 11/14/17 Pct Recovery = 79% Analysis Date = 11/14/17 Pct Recovery = 79% Analysis Date = 11/04/17 Pct Recovery = 79% Analysis Date = 11/04/17 Pct Recovery = 79% Analysis Date = 10/25/17 Pct Recovery = 78% Analysis Date = 10/25/17 Pct Recovery = 78% Analysis Date = 10/15/17 Pct Recovery = 78% Analysis Date = 10/15/17 Pct Recovery = 78% Analysis Date = 10/05/17 Pct Recovery = 78% Analysis Date = 10/05/17 Pct Recovery = 78% Analysis Date = 09/25/17 Pct Recovery = 78% Analysis Date = 09/25/17 Pct Recovery = 78% Analysis Date = 09/15/17 Pct Recovery = 78% Analysis Date = 09/15/17 Pct Recovery = 78% Analysis Date = 09/05/17 Pct Recovery = 77% Analysis Date = 09/05/17 Pct Recovery = 77% Analysis Date = 08/27/17 Pct Recovery = 77% Analysis Date = 08/27/17 Pct Recovery = 77% Analysis Date = 08/17/17 Pct Recovery = 77% Analysis Date = 08/17/17 Pct Recovery = 77% Analysis Date = 08/07/17 Pct Recovery = 77% Analysis Date = 08/07/17 Pct Recovery = 77% Analysis Date = 07/28/17 Pct Recovery = 76% Analysis Date = 07/28/17 Pct Recovery = 76% Analysis Date = 07/18/17 Pct Recovery = 76% Analysis Date = 07/18/17 Pct Recovery = 76% Analysis Date = 07/08/17 Pct Recovery = 76% Analysis Date = 07/08/17 Pct Recovery = 76% Analysis Date = 06/28/17 Pct Recovery = 76% Analysis Date = 06/28/17 Pct Recovery = 76% Analysis Date = 06/18/17 Pct Recovery = 75% Analysis Date = 06/18/17 Pct Recovery = 75% Analysis Date = 06/08/17 Pct Recovery = 75% Analysis Date = 06/08/17 Pct Recovery = 75% Analysis Date = 05/29/17 Pct Recovery = 75% Analysis Date = 05/29/17 Pct Recovery = 75% Analysis Date = 05/20/17 Pct Recovery = 75% Analysis Date = 05/20/17 Pct Recovery = 75% Analysis Date = 05/10/17 Pct Recovery = 74% Analysis Date = 05/10/17 Pct Recovery = 74% Analysis Date = 04/30/17 Pct Recovery = 74% Analysis Date = 04/30/17 Pct Recovery = 74% Analysis Date = 04/20/17 Pct Recovery = 74% Analysis Date = 04/20/17 Pct Recovery = 74% Analysis Date = 04/10/17 Pct Recovery = 74% Analysis Date = 04/10/17 Pct Recovery = 74% Analysis Date = 03/31/17 Pct Recovery = 73% Analysis Date = 03/31/17 Pct Recovery = 73% Analysis Date = 03/21/17 Pct Recovery = 73% Analysis Date = 03/21/17 Pct Recovery = 73% Analysis Date = 03/11/17 Pct Recovery = 73% Analysis Date = 03/11/17 Pct Recovery = 73% Analysis Date = 03/01/17 Pct Recovery = 73% Analysis Date = 03/01/17 Pct Recovery = 73% Analysis Date = 02/19/17 Pct Recovery = 72% Analysis Date = 02/19/17 Pct Recovery = 72% Analysis Date = 02/10/17 Pct Recovery = 72% Analysis Date = 02/10/17 Pct Recovery = 72% Analysis Date = 01/31/17 Pct Recovery = 72% Analysis Date = 01/31/17 Pct Recovery = 72% Analysis Date = 01/21/17 Pct Recovery = 72% Analysis Date = 01/21/17 Pct Recovery = 72% Analysis Date = 01/11/17 Pct Recovery = 71% Analysis Date = 01/11/17 Pct Recovery = 71% Analysis Date = 01/01/17 Pct Recovery = 71% Analysis Date = 01/01/17 Pct Recovery = 71% Analysis Date = 12/22/16 Pct Recovery = 71% Analysis Date = 12/22/16 Pct Recovery = 71% Analysis Date = 12/12/16 Pct Recovery = 70% Analysis Date = 12/12/16 Pct Recovery = 70% Analysis Date = 12/02/16 Pct Recovery = 70% Analysis Date = 12/02/16 Pct Recovery = 70% Analysis Date = 11/22/16 Pct Recovery = 70% Analysis Date = 11/22/16 Pct Recovery = 70% Analysis Date = 11/12/16 Pct Recovery = 70% Analysis Date = 11/12/16 Pct Recovery = 70% Analysis Date = 11/03/16 Pct Recovery = 69% Analysis Date = 11/03/16 Pct Recovery = 69% Analysis Date = 10/24/16 Pct Recovery = 69% Analysis Date = 10/24/16 Pct Recovery = 69% Analysis Date = 10/14/16 Pct Recovery = 69% Analysis Date = 10/14/16 Pct Recovery = 69% Analysis Date = 10/04/16 Pct Recovery = 68% Analysis Date = 10/04/16 Pct Recovery = 68% Analysis Date = 09/24/16 Pct Recovery = 68% Analysis Date = 09/24/16 Pct Recovery = 68% Analysis Date = 09/14/16 Pct Recovery = 68% Analysis Date = 09/14/16 Pct Recovery = 68% Analysis Date = 09/04/16 Pct Recovery = 68% Analysis Date = 09/04/16 Pct Recovery = 68% Analysis Date = 08/25/16 Pct Recovery = 67% Analysis Date = 08/25/16 Pct Recovery = 67% Analysis Date = 08/15/16 Pct Recovery = 67% Analysis Date = 08/15/16 Pct Recovery = 67% Analysis Date = 08/05/16 Pct Recovery = 67% Analysis Date = 08/05/16 Pct Recovery = 67% Analysis Date = 07/27/16 Pct Recovery = 66% Analysis Date = 07/27/16 Pct Recovery = 66% Analysis Date = 07/17/16 Pct Recovery = 66% Analysis Date = 07/17/16 Pct Recovery = 66% Analysis Date = 07/07/16 Pct Recovery = 65% Analysis Date = 07/07/16 Pct Recovery = 65% Analysis Date = 06/27/16 Pct Recovery = 65% Analysis Date = 06/27/16 Pct Recovery = 65% Analysis Date = 06/17/16 Pct Recovery = 65% Analysis Date = 06/17/16 Pct Recovery = 65% Analysis Date = 06/07/16 Pct Recovery = 64% Analysis Date = 06/07/16 Pct Recovery = 64% Analysis Date = 05/28/16 Pct Recovery = 64% Analysis Date = 05/28/16 Pct Recovery = 64% Analysis Date = 05/18/16 Pct Recovery = 64% Analysis Date = 05/18/16 Pct Recovery = 64% Analysis Date = 05/08/16 Pct Recovery = 63% Analysis Date = 05/08/16 Pct Recovery = 63% Analysis Date = 04/28/16 Pct Recovery = 63% Analysis Date = 04/28/16 Pct Recovery = 63% Analysis Date = 04/19/16 Pct Recovery = 62% Analysis Date = 04/19/16 Pct Recovery = 62% Analysis Date = 04/09/16 Pct Recovery = 62% Analysis Date = 04/09/16 Pct Recovery = 62% Analysis Date = 03/30/16 Pct Recovery = 62% Analysis Date = 03/30/16 Pct Recovery = 62% Analysis Date = 03/20/16 Pct Recovery = 61% Analysis Date = 03/20/16 Pct Recovery = 61% Analysis Date = 03/10/16 Pct Recovery = 61% Analysis Date = 03/10/16 Pct Recovery = 61% Analysis Date = 02/29/16 Pct Recovery = 61% Analysis Date = 02/29/16 Pct Recovery = 61% Analysis Date = 02/19/16 Pct Recovery = 60% Analysis Date = 02/19/16 Pct Recovery = 60% Analysis Date = 02/09/16 Pct Recovery = 60% Analysis Date = 02/09/16 Pct Recovery = 60% Analysis Date = 01/30/16 Pct Recovery = 60% Analysis Date = 01/30/16 Pct Recovery = 60% Analysis Date = 01/20/16 Pct Recovery = 59% Analysis Date = 01/20/16 Pct Recovery = 59% Analysis Date = 01/11/16 Pct Recovery = 59% Analysis Date = 01/11/16 Pct Recovery = 59% Analysis Date = 01/01/16 Pct Recovery = 59% Analysis Date = 01/01/16 Pct Recovery = 59% Analysis Date = 12/22/15 Pct Recovery = 59% Analysis Date = 12/22/15 Pct Recovery = 59% Analysis Date = 12/12/15 Pct Recovery = 59% Analysis Date = 12/12/15 Pct Recovery = 59% Analysis Date = 12/02/15 Pct Recovery = 58% Analysis Date = 12/02/15 Pct Recovery = 58% Analysis Date = 11/22/15 Pct Recovery = 58% Analysis Date = 11/22/15 Pct Recovery = 58% Analysis Date = 11/12/15 Pct Recovery = 58% Analysis Date = 11/12/15 Pct Recovery = 58% Analysis Date = 11/02/15 Pct Recovery = 58% Analysis Date = 11/02/15 Pct Recovery = 58% Analysis Date = 10/23/15 Pct Recovery = 58% Analysis Date = 10/23/15 Pct Recovery = 58% Analysis Date = 10/13/15 Pct Recovery = 57% Analysis Date = 10/13/15 Pct Recovery = 57% Analysis Date = 10/04/15 Pct Recovery = 57% Analysis Date = 10/04/15 Pct Recovery = 57% Analysis Date = 09/24/15 Pct Recovery = 57% Analysis Date = 09/24/15 Pct Recovery = 57% Analysis Date = 09/14/15 Pct Recovery = 57% Analysis Date = 09/14/15 Pct Recovery = 57% Analysis Date = 09/04/15 Pct Recovery = 57% Analysis Date = 09/04/15 Pct Recovery = 57% Analysis Date = 08/25/15 Pct Recovery = 56% Analysis Date = 08/25/15 Pct Recovery = 56% Analysis Date = 08/15/15 Pct Recovery = 56% Analysis Date = 08/15/15 Pct Recovery = 56% Analysis Date = 08/05/15 Pct Recovery = 56% Analysis Date = 08/05/15 Pct Recovery = 56% Analysis Date = 07/26/15 Pct Recovery = 56% Analysis Date = 07/26/15 Pct Recovery = 56% Analysis Date = 07/16/15 Pct Recovery = 56% Analysis Date = 07/16/15 Pct Recovery = 56% Analysis Date = 07/06/15 Pct Recovery = 55% Analysis Date = 07/06/15 Pct Recovery = 55% Analysis Date = 06/27/15 Pct Recovery = 55% Analysis Date = 06/27/15 Pct Recovery = 55% Analysis Date = 06/17/15 Pct Recovery = 55% Analysis Date = 06/17/15 Pct Recovery = 55% Analysis Date = 06/07/15 Pct Recovery = 55% Analysis Date = 06/07/15 Pct Recovery = 55% Analysis Date = 05/28/15 Pct Recovery = 55% Analysis Date = 05/28/15 Pct Recovery = 55% Analysis Date = 05/18/15 Pct Recovery = 54% Analysis Date = 05/18/15 Pct Recovery = 54% Analysis Date = 05/08/15 Pct Recovery = 54% Analysis Date = 05/08/15 Pct Recovery = 54% Analysis Date = 04/28/15 Pct Recovery = 54% Analysis Date = 04/28/15 Pct Recovery = 54% Analysis Date = 04/18/15 Pct Recovery = 54% Analysis Date = 04/18/15 Pct Recovery = 54% Analysis Date = 04/08/15 Pct Recovery = 54% Analysis Date = 04/08/15 Pct Recovery = 54% Analysis Date = 03/29/15 Pct Recovery = 54% Analysis Date = 03/29/15 Pct Recovery = 54% Analysis Date = 03/20/15 Pct Recovery = 54% Analysis Date = 03/20/15 Pct Recovery = 54% Analysis Date = 03/10/15 Pct Recovery = 54% Analysis Date = 03/10/15 Pct Recovery = 54% Analysis Date = 02/28/15 Pct Recovery = 54% Analysis Date = 02/28/15 Pct Recovery = 54% Analysis Date = 02/18/15 Pct Recovery = 54% Analysis Date = 02/18/15 Pct Recovery = 54% Analysis Date = 02/08/15 Pct Recovery = 54% Analysis Date = 02/08/15 Pct Recovery = 54% Analysis Date = 01/29/15 Pct Recovery = 54% Analysis Date = 01/29/15 Pct Recovery = 54% Analysis Date = 01/19/15 Pct Recovery = 54% Analysis Date = 01/19/15 Pct Recovery = 54% Analysis Date = 01/09/15 Pct Recovery = 54% Analysis Date = 01/09/15 Pct Recovery = 54% Analysis Date = 12/30/14 Pct Recovery = 54% Analysis Date = 12/30/14 Pct Recovery = 54% Analysis Date = 12/20/14 Pct Recovery = 54% Analysis Date = 12/20/14 Pct Recovery = 54% Analysis Date = 12/11/14 Pct Recovery = 54% Analysis Date = 12/11/14 Pct Recovery = 54% Analysis Date = 12/01/14 Pct Recovery = 54% Analysis Date = 12/01/14 Pct Recovery = 54% Analysis Date = 11/21/14 Pct Recovery = 54% Analysis Date = 11/21/14 Pct Recovery = 54% Analysis Date = 11/11/14 Pct Recovery = 54% Analysis Date = 11/11/14 Pct Recovery = 54% Analysis Date = 11/01/14 Pct Recovery = 55% Analysis Date = 11/01/14 Pct Recovery = 55% Analysis Date = 10/22/14 Pct Recovery = 55% Analysis Date = 10/22/14 Pct Recovery = 55% Analysis Date = 10/12/14 Pct Recovery = 55% Analysis Date = 10/12/14 Pct Recovery = 55% Analysis Date = 10/02/14 Pct Recovery = 55% Analysis Date = 10/02/14 Pct Recovery = 55% Analysis Date = 09/22/14 Pct Recovery = 55% Analysis Date = 09/22/14 Pct Recovery = 55% Analysis Date = 09/12/14 Pct Recovery = 56% Analysis Date = 09/12/14 Pct Recovery = 56% Analysis Date = 09/03/14 Pct Recovery = 56% Analysis Date = 09/03/14 Pct Recovery = 56% Analysis Date = 08/24/14 Pct Recovery = 56% Analysis Date = 08/24/14 Pct Recovery = 56% Analysis Date = 08/14/14 Pct Recovery = 56% Analysis Date = 08/14/14 Pct Recovery = 56% Analysis Date = 08/04/14 Pct Recovery = 57% Analysis Date = 08/04/14 Pct Recovery = 57% Analysis Date = 07/25/14 Pct Recovery = 57% Analysis Date = 07/25/14 Pct Recovery = 57% Analysis Date = 07/15/14 Pct Recovery = 57% Analysis Date = 07/15/14 Pct Recovery = 57% Analysis Date = 07/05/14 Pct Recovery = 57% Analysis Date = 07/05/14 Pct Recovery = 57% Analysis Date = 06/25/14 Pct Recovery = 57% Analysis Date = 06/25/14 Pct Recovery = 57% Analysis Date = 06/15/14 Pct Recovery = 57% Analysis Date = 06/15/14 Pct Recovery = 57% Analysis Date = 06/05/14 Pct Recovery = 57% Analysis Date = 06/05/14 Pct Recovery = 57% Analysis Date = 05/27/14 Pct Recovery = 57% Analysis Date = 05/27/14 Pct Recovery = 57% Analysis Date = 05/17/14 Pct Recovery = 57% Analysis Date = 05/17/14 Pct Recovery = 57% Analysis Date = 05/07/14 Pct Recovery = 57% Analysis Date = 05/07/14 Pct Recovery = 57% Analysis Date = 04/27/14 Pct Recovery = 57% Analysis Date = 04/27/14 Pct Recovery = 57% Analysis Date = 04/17/14 Pct Recovery = 57% Analysis Date = 04/17/14 Pct Recovery = 57% Analysis Date = 04/07/14 Pct Recovery = 57% Analysis Date = 04/07/14 Pct Recovery = 57% Analysis Date = 03/28/14 Pct Recovery = 57% Analysis Date = 03/28/14 Pct Recovery = 57% Analysis Date = 03/18/14 Pct Recovery = 57% Analysis Date = 03/18/14 Pct Recovery = 57% Analysis Date = 03/08/14 Pct Recovery = 57% Analysis Date = 03/08/14 Pct Recovery = 57% Analysis Date = 02/26/14 Pct Recovery = 57% Analysis Date = 02/26/14 Pct Recovery = 57% Analysis Date = 02/17/14 Pct Recovery = 57% Analysis Date = 02/17/14 Pct Recovery = 57% Analysis Date = 02/07/14 Pct Recovery = 57% Analysis Date = 02/07/14 Pct Recovery = 57% Analysis Date = 01/28/14 Pct Recovery = 57% Analysis Date = 01/28/14 Pct Recovery = 57% Analysis Date = 01/18/14 Pct Recovery = 56% Analysis Date = 01/18/14 Pct Recovery = 56% Analysis Date = 01/08/14 Pct Recovery = 56% Analysis Date = 01/08/14 Pct Recovery = 56% Analysis Date = 12/29/13 Pct Recovery = 56% Analysis Date = 12/29/13 Pct Recovery = 56% Analysis Date = 12/19/13 Pct Recovery = 56% Analysis Date = 12/19/13 Pct Recovery = 56% Analysis Date = 12/09/13 Pct Recovery = 56% Analysis Date = 12/09/13 Pct Recovery = 56% Analysis Date = 11/29/13 Pct Recovery = 56% Analysis Date = 11/29/13 Pct Recovery = 56% Analysis Date = 11/19/13 Pct Recovery = 56% Analysis Date = 11/19/13 Pct Recovery = 56% Analysis Date = 11/10/13 Pct Recovery = 56% Analysis Date = 11/10/13 Pct Recovery = 56% Analysis Date = 10/31/13 Pct Recovery = 56% Analysis Date = 10/31/13 Pct Recovery = 56% Analysis Date = 10/21/13 Pct Recovery = 56% Analysis Date = 10/21/13 Pct Recovery = 56% Analysis Date = 10/11/13 Pct Recovery = 55% Analysis Date = 10/11/13 Pct Recovery = 55% Analysis Date = 10/01/13 Pct Recovery = 55% Analysis Date = 10/01/13 Pct Recovery = 55% Analysis Date = 09/21/13 Pct Recovery = 55% Analysis Date = 09/21/13 Pct Recovery = 55% Analysis Date = 09/11/13 Pct Recovery = 55% Analysis Date = 09/11/13 Pct Recovery = 55% Analysis Date = 09/01/13 Pct Recovery = 55% Analysis Date = 09/01/13 Pct Recovery = 55% Analysis Date = 08/22/13 Pct Recovery = 55% Analysis Date = 08/22/13 Pct Recovery = 55% Analysis Date = 08/12/13 Pct Recovery = 55% Analysis Date = 08/12/13 Pct Recovery = 55% Analysis Date = 08/03/13 Pct Recovery = 54% Analysis Date = 08/03/13 Pct Recovery = 54% Analysis Date = 07/24/13 Pct Recovery = 54% Analysis Date = 07/24/13 Pct Recovery = 54% Analysis Date = 07/14/13 Pct Recovery = 54% Analysis Date = 07/14/13 Pct Recovery = 54% Analysis Date = 07/04/13 Pct Recovery = 54% Analysis Date = 07/04/13 Pct Recovery = 54% Analysis Date = 06/24/13 Pct Recovery = 54% Analysis Date = 06/24/13 Pct Recovery = 54% Analysis Date = 06/14/13 Pct Recovery = 54% Analysis Date = 06/14/13 Pct Recovery = 54% Analysis Date = 06/04/13 Pct Recovery = 54% Analysis Date = 06/04/13 Pct Recovery = 54% Analysis Date = 05/25/13 Pct Recovery = 53% Analysis Date = 05/25/13 Pct Recovery = 53% Analysis Date = 05/15/13 Pct Recovery = 53% Analysis Date = 05/15/13 Pct Recovery = 53% Analysis Date = 05/05/13 Pct Recovery = 53% Analysis Date = 05/05/13 Pct Recovery = 53% Analysis Date = 04/26/13 Pct Recovery = 53% Analysis Date = 04/26/13 Pct Recovery = 53% Analysis Date = 04/16/13 Pct Recovery = 53% Analysis Date = 04/16/13 Pct Recovery = 53% Analysis Date = 04/06/13 Pct Recovery = 53% Analysis Date = 04/06/13 Pct Recovery = 53% Analysis Date = 03/27/13 Pct Recovery = 52% Analysis Date = 03/27/13 Pct Recovery = 52% Analysis Date = 03/17/13 Pct Recovery = 52% Analysis Date = 03/17/13 Pct Recovery = 52% Analysis Date = 03/07/13 Pct Recovery = 52% Analysis Date = 03/07/13 Pct Recovery = 52% Analysis Date = 02/25/13 Pct Recovery = 52% Analysis Date = 02/25/13 Pct Recovery = 52% Analysis Date = 02/15/13 Pct Recovery = 52% Analysis Date = 02/15/13 Pct Recovery = 52% Analysis Date = 02/05/13 Pct Recovery = 51% Analysis Date = 02/05/13 Pct Recovery = 51% Analysis Date = 01/26/13 Pct Recovery = 51% Analysis Date = 01/26/13 Pct Recovery = 51% Analysis Date = 01/17/13 Pct Recovery = 51% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
TERBUFOS

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 73 63% 18% 60% 19%
Total 73 63% 18% 60% 19%

Sample Statistics
TERBUFOS

Characteristic N % % Basis
Plotted 73 94% Spiked
Estimated Values 0 0% Spiked
Deleted Values 5 4% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 81 .  
False Negatives 5 6% 5 out of 78
Not Spiked 53 .  
False Positives 0 0% 0 out of 51

OBSP Determination:
TERBUFOS-O-ANALOGUE SULFONE
METHOD: 2033 , TESTIDCODE: 61674GCM39

Laboratory ID = 20172510330 Lab Value = 0.187 Expected Conc. = 0.301 Report level label = 0.045 Pct Recovery = 62% Analysis Date = 12/29/17 SpikeMix = ChemService 6537100: 100 µl & Abs 071817Pest: 100 µl SpecificMix = 071817Pest Laboratory ID = 20140100085 Lab Value = 0.178 Expected Conc. = 0.2 Report level label = 0.045 Pct Recovery = 89% Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl SpecificMix = 10802AL Laboratory ID = 20133310030 Lab Value = 0.159 Expected Conc. = 0.2 Report level label = 0.045 Pct Recovery = 79% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl SpecificMix = 10802AL Laboratory ID = 20132690010 Lab Value = 0.128 Expected Conc. = 0.2 Report level label = 0.045 Pct Recovery = 64% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl SpecificMix = 10802AL Laboratory ID = 20140860102 Lab Value = 0.049 Expected Conc. = 0.1 Report level label = 0.045 Pct Recovery = 49% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 10802AL Laboratory ID = 20140730138 Lab Value = 0.027 Expected Conc. = 0.1 Report level label = 0.045 Pct Recovery = 26% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 10802AL Laboratory ID = 20140510043 Lab Value = 0.039 Expected Conc. = 0.1 Report level label = 0.045 Pct Recovery = 38% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 10802AL Laboratory ID = 20140230082 Lab Value = 0.060 Expected Conc. = 0.1 Report level label = 0.045 Pct Recovery = 60% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl SpecificMix = 10802AL Laboratory ID = 20133580036 Lab Value = 0.057 Expected Conc. = 0.1 Report level label = 0.045 Pct Recovery = 57% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 10802AL Laboratory ID = 20133190012 Lab Value = 0.089 Expected Conc. = 0.1 Report level label = 0.045 Pct Recovery = 89% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 10802AL Laboratory ID = 20132560001 Lab Value = 0.053 Expected Conc. = 0.1 Report level label = 0.045 Pct Recovery = 53% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl SpecificMix = 10802AL Laboratory ID = 20172780018 Lab Value = 0.054 Expected Conc. = 0.0903 Report level label = 0.045 Pct Recovery = 59% Analysis Date = 02/08/18 SpikeMix = ChemService 6537100: 30 µl & Abs 071817Pest: 30 µl SpecificMix = 071817Pest Laboratory ID = 20130940097 Lab Value = 0.041 Expected Conc. = 0.0535 Report level label = 0.045 Pct Recovery = 76% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = 0507-12-04.2 Laboratory ID = 20123560092 Lab Value = 0.037 Expected Conc. = 0.0535 Report level label = 0.045 Pct Recovery = 70% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = 0507-12-04.2 Laboratory ID = 20133400002 Lab Value = 0.034 Expected Conc. = 0.05 Report level label = 0.045 Pct Recovery = 68% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = 10802AL Laboratory ID = 20132910008 Lab Value = 0.026 Expected Conc. = 0.05 Report level label = 0.045 Pct Recovery = 51% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = 10802AL Laboratory ID = 20132420001 Lab Value = 0.035 Expected Conc. = 0.05 Report level label = 0.045 Pct Recovery = 69% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl SpecificMix = 10802AL Laboratory ID = 20130510051 Lab Value = 0.023 Expected Conc. = 0.0214 Report level label = 0.045 Pct Recovery = 107% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl SpecificMix = 0507-12-04.2 Analysis Date = 02/08/18 Pct Recovery = 61% Analysis Date = 01/29/18 Pct Recovery = 61% Analysis Date = 01/29/18 Pct Recovery = 61% Analysis Date = 01/20/18 Pct Recovery = 61% Analysis Date = 01/20/18 Pct Recovery = 61% Analysis Date = 01/11/18 Pct Recovery = 60% Analysis Date = 01/11/18 Pct Recovery = 60% Analysis Date = 01/02/18 Pct Recovery = 60% Analysis Date = 01/02/18 Pct Recovery = 60% Analysis Date = 12/23/17 Pct Recovery = 60% Analysis Date = 12/23/17 Pct Recovery = 60% Analysis Date = 12/14/17 Pct Recovery = 60% Analysis Date = 12/14/17 Pct Recovery = 60% Analysis Date = 12/05/17 Pct Recovery = 60% Analysis Date = 12/05/17 Pct Recovery = 60% Analysis Date = 11/26/17 Pct Recovery = 60% Analysis Date = 11/26/17 Pct Recovery = 60% Analysis Date = 11/16/17 Pct Recovery = 59% Analysis Date = 11/16/17 Pct Recovery = 59% Analysis Date = 11/07/17 Pct Recovery = 59% Analysis Date = 11/07/17 Pct Recovery = 59% Analysis Date = 10/29/17 Pct Recovery = 59% Analysis Date = 10/29/17 Pct Recovery = 59% Analysis Date = 10/20/17 Pct Recovery = 59% Analysis Date = 10/20/17 Pct Recovery = 59% Analysis Date = 10/10/17 Pct Recovery = 59% Analysis Date = 10/10/17 Pct Recovery = 59% Analysis Date = 10/01/17 Pct Recovery = 59% Analysis Date = 10/01/17 Pct Recovery = 59% Analysis Date = 09/22/17 Pct Recovery = 58% Analysis Date = 09/22/17 Pct Recovery = 58% Analysis Date = 09/13/17 Pct Recovery = 58% Analysis Date = 09/13/17 Pct Recovery = 58% Analysis Date = 09/03/17 Pct Recovery = 58% Analysis Date = 09/03/17 Pct Recovery = 58% Analysis Date = 08/25/17 Pct Recovery = 58% Analysis Date = 08/25/17 Pct Recovery = 58% Analysis Date = 08/16/17 Pct Recovery = 58% Analysis Date = 08/16/17 Pct Recovery = 58% Analysis Date = 08/07/17 Pct Recovery = 57% Analysis Date = 08/07/17 Pct Recovery = 57% Analysis Date = 07/28/17 Pct Recovery = 57% Analysis Date = 07/28/17 Pct Recovery = 57% Analysis Date = 07/19/17 Pct Recovery = 57% Analysis Date = 07/19/17 Pct Recovery = 57% Analysis Date = 07/10/17 Pct Recovery = 57% Analysis Date = 07/10/17 Pct Recovery = 57% Analysis Date = 07/01/17 Pct Recovery = 57% Analysis Date = 07/01/17 Pct Recovery = 57% Analysis Date = 06/21/17 Pct Recovery = 57% Analysis Date = 06/21/17 Pct Recovery = 57% Analysis Date = 06/12/17 Pct Recovery = 56% Analysis Date = 06/12/17 Pct Recovery = 56% Analysis Date = 06/03/17 Pct Recovery = 56% Analysis Date = 06/03/17 Pct Recovery = 56% Analysis Date = 05/25/17 Pct Recovery = 56% Analysis Date = 05/25/17 Pct Recovery = 56% Analysis Date = 05/15/17 Pct Recovery = 56% Analysis Date = 05/15/17 Pct Recovery = 56% Analysis Date = 05/06/17 Pct Recovery = 56% Analysis Date = 05/06/17 Pct Recovery = 56% Analysis Date = 04/27/17 Pct Recovery = 55% Analysis Date = 04/27/17 Pct Recovery = 55% Analysis Date = 04/18/17 Pct Recovery = 55% Analysis Date = 04/18/17 Pct Recovery = 55% Analysis Date = 04/08/17 Pct Recovery = 55% Analysis Date = 04/08/17 Pct Recovery = 55% Analysis Date = 03/30/17 Pct Recovery = 55% Analysis Date = 03/30/17 Pct Recovery = 55% Analysis Date = 03/21/17 Pct Recovery = 55% Analysis Date = 03/21/17 Pct Recovery = 55% Analysis Date = 03/12/17 Pct Recovery = 55% Analysis Date = 03/12/17 Pct Recovery = 55% Analysis Date = 03/02/17 Pct Recovery = 54% Analysis Date = 03/02/17 Pct Recovery = 54% Analysis Date = 02/21/17 Pct Recovery = 54% Analysis Date = 02/21/17 Pct Recovery = 54% Analysis Date = 02/12/17 Pct Recovery = 54% Analysis Date = 02/12/17 Pct Recovery = 54% Analysis Date = 02/03/17 Pct Recovery = 54% Analysis Date = 02/03/17 Pct Recovery = 54% Analysis Date = 01/24/17 Pct Recovery = 54% Analysis Date = 01/24/17 Pct Recovery = 54% Analysis Date = 01/15/17 Pct Recovery = 53% Analysis Date = 01/15/17 Pct Recovery = 53% Analysis Date = 01/06/17 Pct Recovery = 53% Analysis Date = 01/06/17 Pct Recovery = 53% Analysis Date = 12/28/16 Pct Recovery = 53% Analysis Date = 12/28/16 Pct Recovery = 53% Analysis Date = 12/18/16 Pct Recovery = 53% Analysis Date = 12/18/16 Pct Recovery = 53% Analysis Date = 12/09/16 Pct Recovery = 53% Analysis Date = 12/09/16 Pct Recovery = 53% Analysis Date = 11/30/16 Pct Recovery = 53% Analysis Date = 11/30/16 Pct Recovery = 53% Analysis Date = 11/21/16 Pct Recovery = 52% Analysis Date = 11/21/16 Pct Recovery = 52% Analysis Date = 11/11/16 Pct Recovery = 52% Analysis Date = 11/11/16 Pct Recovery = 52% Analysis Date = 11/02/16 Pct Recovery = 52% Analysis Date = 11/02/16 Pct Recovery = 52% Analysis Date = 10/24/16 Pct Recovery = 52% Analysis Date = 10/24/16 Pct Recovery = 52% Analysis Date = 10/15/16 Pct Recovery = 52% Analysis Date = 10/15/16 Pct Recovery = 52% Analysis Date = 10/05/16 Pct Recovery = 51% Analysis Date = 10/05/16 Pct Recovery = 51% Analysis Date = 09/26/16 Pct Recovery = 51% Analysis Date = 09/26/16 Pct Recovery = 51% Analysis Date = 09/17/16 Pct Recovery = 51% Analysis Date = 09/17/16 Pct Recovery = 51% Analysis Date = 09/08/16 Pct Recovery = 51% Analysis Date = 09/08/16 Pct Recovery = 51% Analysis Date = 08/29/16 Pct Recovery = 51% Analysis Date = 08/29/16 Pct Recovery = 51% Analysis Date = 08/20/16 Pct Recovery = 51% Analysis Date = 08/20/16 Pct Recovery = 51% Analysis Date = 08/11/16 Pct Recovery = 50% Analysis Date = 08/11/16 Pct Recovery = 50% Analysis Date = 08/02/16 Pct Recovery = 50% Analysis Date = 08/02/16 Pct Recovery = 50% Analysis Date = 07/23/16 Pct Recovery = 50% Analysis Date = 07/23/16 Pct Recovery = 50% Analysis Date = 07/14/16 Pct Recovery = 50% Analysis Date = 07/14/16 Pct Recovery = 50% Analysis Date = 07/05/16 Pct Recovery = 50% Analysis Date = 07/05/16 Pct Recovery = 50% Analysis Date = 06/26/16 Pct Recovery = 50% Analysis Date = 06/26/16 Pct Recovery = 50% Analysis Date = 06/16/16 Pct Recovery = 49% Analysis Date = 06/16/16 Pct Recovery = 49% Analysis Date = 06/07/16 Pct Recovery = 49% Analysis Date = 06/07/16 Pct Recovery = 49% Analysis Date = 05/29/16 Pct Recovery = 49% Analysis Date = 05/29/16 Pct Recovery = 49% Analysis Date = 05/20/16 Pct Recovery = 49% Analysis Date = 05/20/16 Pct Recovery = 49% Analysis Date = 05/10/16 Pct Recovery = 49% Analysis Date = 05/10/16 Pct Recovery = 49% Analysis Date = 05/01/16 Pct Recovery = 48% Analysis Date = 05/01/16 Pct Recovery = 48% Analysis Date = 04/22/16 Pct Recovery = 48% Analysis Date = 04/22/16 Pct Recovery = 48% Analysis Date = 04/13/16 Pct Recovery = 48% Analysis Date = 04/13/16 Pct Recovery = 48% Analysis Date = 04/03/16 Pct Recovery = 48% Analysis Date = 04/03/16 Pct Recovery = 48% Analysis Date = 03/25/16 Pct Recovery = 48% Analysis Date = 03/25/16 Pct Recovery = 48% Analysis Date = 03/16/16 Pct Recovery = 48% Analysis Date = 03/16/16 Pct Recovery = 48% Analysis Date = 03/07/16 Pct Recovery = 47% Analysis Date = 03/07/16 Pct Recovery = 47% Analysis Date = 02/26/16 Pct Recovery = 47% Analysis Date = 02/26/16 Pct Recovery = 47% Analysis Date = 02/17/16 Pct Recovery = 47% Analysis Date = 02/17/16 Pct Recovery = 47% Analysis Date = 02/08/16 Pct Recovery = 47% Analysis Date = 02/08/16 Pct Recovery = 47% Analysis Date = 01/30/16 Pct Recovery = 47% Analysis Date = 01/30/16 Pct Recovery = 47% Analysis Date = 01/20/16 Pct Recovery = 46% Analysis Date = 01/20/16 Pct Recovery = 46% Analysis Date = 01/11/16 Pct Recovery = 46% Analysis Date = 01/11/16 Pct Recovery = 46% Analysis Date = 01/02/16 Pct Recovery = 46% Analysis Date = 01/02/16 Pct Recovery = 46% Analysis Date = 12/24/15 Pct Recovery = 46% Analysis Date = 12/24/15 Pct Recovery = 46% Analysis Date = 12/14/15 Pct Recovery = 46% Analysis Date = 12/14/15 Pct Recovery = 46% Analysis Date = 12/05/15 Pct Recovery = 46% Analysis Date = 12/05/15 Pct Recovery = 46% Analysis Date = 11/26/15 Pct Recovery = 45% Analysis Date = 11/26/15 Pct Recovery = 45% Analysis Date = 11/17/15 Pct Recovery = 45% Analysis Date = 11/17/15 Pct Recovery = 45% Analysis Date = 11/07/15 Pct Recovery = 45% Analysis Date = 11/07/15 Pct Recovery = 45% Analysis Date = 10/29/15 Pct Recovery = 45% Analysis Date = 10/29/15 Pct Recovery = 45% Analysis Date = 10/20/15 Pct Recovery = 45% Analysis Date = 10/20/15 Pct Recovery = 45% Analysis Date = 10/11/15 Pct Recovery = 44% Analysis Date = 10/11/15 Pct Recovery = 44% Analysis Date = 10/01/15 Pct Recovery = 44% Analysis Date = 10/01/15 Pct Recovery = 44% Analysis Date = 09/22/15 Pct Recovery = 44% Analysis Date = 09/22/15 Pct Recovery = 44% Analysis Date = 09/13/15 Pct Recovery = 44% Analysis Date = 09/13/15 Pct Recovery = 44% Analysis Date = 09/04/15 Pct Recovery = 44% Analysis Date = 09/04/15 Pct Recovery = 44% Analysis Date = 08/25/15 Pct Recovery = 44% Analysis Date = 08/25/15 Pct Recovery = 44% Analysis Date = 08/16/15 Pct Recovery = 43% Analysis Date = 08/16/15 Pct Recovery = 43% Analysis Date = 08/07/15 Pct Recovery = 43% Analysis Date = 08/07/15 Pct Recovery = 43% Analysis Date = 07/29/15 Pct Recovery = 43% Analysis Date = 07/29/15 Pct Recovery = 43% Analysis Date = 07/19/15 Pct Recovery = 43% Analysis Date = 07/19/15 Pct Recovery = 43% Analysis Date = 07/10/15 Pct Recovery = 43% Analysis Date = 07/10/15 Pct Recovery = 43% Analysis Date = 07/01/15 Pct Recovery = 42% Analysis Date = 07/01/15 Pct Recovery = 42% Analysis Date = 06/22/15 Pct Recovery = 42% Analysis Date = 06/22/15 Pct Recovery = 42% Analysis Date = 06/12/15 Pct Recovery = 42% Analysis Date = 06/12/15 Pct Recovery = 42% Analysis Date = 06/03/15 Pct Recovery = 42% Analysis Date = 06/03/15 Pct Recovery = 42% Analysis Date = 05/25/15 Pct Recovery = 42% Analysis Date = 05/25/15 Pct Recovery = 42% Analysis Date = 05/16/15 Pct Recovery = 42% Analysis Date = 05/16/15 Pct Recovery = 42% Analysis Date = 05/06/15 Pct Recovery = 41% Analysis Date = 05/06/15 Pct Recovery = 41% Analysis Date = 04/27/15 Pct Recovery = 41% Analysis Date = 04/27/15 Pct Recovery = 41% Analysis Date = 04/18/15 Pct Recovery = 41% Analysis Date = 04/18/15 Pct Recovery = 41% Analysis Date = 04/09/15 Pct Recovery = 41% Analysis Date = 04/09/15 Pct Recovery = 41% Analysis Date = 03/30/15 Pct Recovery = 41% Analysis Date = 03/30/15 Pct Recovery = 41% Analysis Date = 03/21/15 Pct Recovery = 40% Analysis Date = 03/21/15 Pct Recovery = 40% Analysis Date = 03/12/15 Pct Recovery = 40% Analysis Date = 03/12/15 Pct Recovery = 40% Analysis Date = 03/03/15 Pct Recovery = 40% Analysis Date = 03/03/15 Pct Recovery = 40% Analysis Date = 02/21/15 Pct Recovery = 40% Analysis Date = 02/21/15 Pct Recovery = 40% Analysis Date = 02/12/15 Pct Recovery = 40% Analysis Date = 02/12/15 Pct Recovery = 40% Analysis Date = 02/03/15 Pct Recovery = 40% Analysis Date = 02/03/15 Pct Recovery = 40% Analysis Date = 01/25/15 Pct Recovery = 39% Analysis Date = 01/25/15 Pct Recovery = 39% Analysis Date = 01/15/15 Pct Recovery = 39% Analysis Date = 01/15/15 Pct Recovery = 39% Analysis Date = 01/06/15 Pct Recovery = 39% Analysis Date = 01/06/15 Pct Recovery = 39% Analysis Date = 12/28/14 Pct Recovery = 39% Analysis Date = 12/28/14 Pct Recovery = 39% Analysis Date = 12/19/14 Pct Recovery = 39% Analysis Date = 12/19/14 Pct Recovery = 39% Analysis Date = 12/09/14 Pct Recovery = 39% Analysis Date = 12/09/14 Pct Recovery = 39% Analysis Date = 11/30/14 Pct Recovery = 38% Analysis Date = 11/30/14 Pct Recovery = 38% Analysis Date = 11/21/14 Pct Recovery = 38% Analysis Date = 11/21/14 Pct Recovery = 38% Analysis Date = 11/12/14 Pct Recovery = 38% Analysis Date = 11/12/14 Pct Recovery = 38% Analysis Date = 11/02/14 Pct Recovery = 38% Analysis Date = 11/02/14 Pct Recovery = 38% Analysis Date = 10/24/14 Pct Recovery = 38% Analysis Date = 10/24/14 Pct Recovery = 38% Analysis Date = 10/15/14 Pct Recovery = 37% Analysis Date = 10/15/14 Pct Recovery = 37% Analysis Date = 10/06/14 Pct Recovery = 37% Analysis Date = 10/06/14 Pct Recovery = 37% Analysis Date = 09/26/14 Pct Recovery = 37% Analysis Date = 09/26/14 Pct Recovery = 37% Analysis Date = 09/17/14 Pct Recovery = 37% Analysis Date = 09/17/14 Pct Recovery = 37% Analysis Date = 09/08/14 Pct Recovery = 37% Analysis Date = 09/08/14 Pct Recovery = 37% Analysis Date = 08/30/14 Pct Recovery = 37% Analysis Date = 08/30/14 Pct Recovery = 37% Analysis Date = 08/20/14 Pct Recovery = 36% Analysis Date = 08/20/14 Pct Recovery = 36% Analysis Date = 08/11/14 Pct Recovery = 36% Analysis Date = 08/11/14 Pct Recovery = 36% Analysis Date = 08/02/14 Pct Recovery = 36% Analysis Date = 08/02/14 Pct Recovery = 36% Analysis Date = 07/24/14 Pct Recovery = 36% Analysis Date = 07/24/14 Pct Recovery = 36% Analysis Date = 07/14/14 Pct Recovery = 36% Analysis Date = 07/14/14 Pct Recovery = 36% Analysis Date = 07/05/14 Pct Recovery = 35% Analysis Date = 07/05/14 Pct Recovery = 35% Analysis Date = 06/26/14 Pct Recovery = 35% Analysis Date = 06/26/14 Pct Recovery = 35% Analysis Date = 06/17/14 Pct Recovery = 35% Analysis Date = 06/17/14 Pct Recovery = 35% Analysis Date = 06/07/14 Pct Recovery = 35% Analysis Date = 06/07/14 Pct Recovery = 35% Analysis Date = 05/29/14 Pct Recovery = 35% Analysis Date = 05/29/14 Pct Recovery = 35% Analysis Date = 05/20/14 Pct Recovery = 35% Analysis Date = 05/20/14 Pct Recovery = 35% Analysis Date = 05/11/14 Pct Recovery = 34% Analysis Date = 05/11/14 Pct Recovery = 34% Analysis Date = 05/01/14 Pct Recovery = 34% Analysis Date = 05/01/14 Pct Recovery = 34% Analysis Date = 04/22/14 Pct Recovery = 34% Analysis Date = 04/22/14 Pct Recovery = 34% Analysis Date = 04/13/14 Pct Recovery = 34% Analysis Date = 04/13/14 Pct Recovery = 34% Analysis Date = 04/04/14 Pct Recovery = 38% Analysis Date = 04/04/14 Pct Recovery = 38% Analysis Date = 03/25/14 Pct Recovery = 41% Analysis Date = 03/25/14 Pct Recovery = 41% Analysis Date = 03/16/14 Pct Recovery = 44% Analysis Date = 03/16/14 Pct Recovery = 44% Analysis Date = 03/07/14 Pct Recovery = 48% Analysis Date = 03/07/14 Pct Recovery = 48% Analysis Date = 02/26/14 Pct Recovery = 51% Analysis Date = 02/26/14 Pct Recovery = 51% Analysis Date = 02/16/14 Pct Recovery = 55% Analysis Date = 02/16/14 Pct Recovery = 55% Analysis Date = 02/07/14 Pct Recovery = 58% Analysis Date = 02/07/14 Pct Recovery = 58% Analysis Date = 01/29/14 Pct Recovery = 61% Analysis Date = 01/29/14 Pct Recovery = 61% Analysis Date = 01/20/14 Pct Recovery = 65% Analysis Date = 01/20/14 Pct Recovery = 65% Analysis Date = 01/10/14 Pct Recovery = 68% Analysis Date = 01/10/14 Pct Recovery = 68% Analysis Date = 01/01/14 Pct Recovery = 69% Analysis Date = 01/01/14 Pct Recovery = 69% Analysis Date = 12/23/13 Pct Recovery = 70% Analysis Date = 12/23/13 Pct Recovery = 70% Analysis Date = 12/14/13 Pct Recovery = 70% Analysis Date = 12/14/13 Pct Recovery = 70% Analysis Date = 12/04/13 Pct Recovery = 71% Analysis Date = 12/04/13 Pct Recovery = 71% Analysis Date = 11/25/13 Pct Recovery = 70% Analysis Date = 11/25/13 Pct Recovery = 70% Analysis Date = 11/16/13 Pct Recovery = 69% Analysis Date = 11/16/13 Pct Recovery = 69% Analysis Date = 11/07/13 Pct Recovery = 68% Analysis Date = 11/07/13 Pct Recovery = 68% Analysis Date = 10/28/13 Pct Recovery = 67% Analysis Date = 10/28/13 Pct Recovery = 67% Analysis Date = 10/19/13 Pct Recovery = 65% Analysis Date = 10/19/13 Pct Recovery = 65% Analysis Date = 10/10/13 Pct Recovery = 64% Analysis Date = 10/10/13 Pct Recovery = 64% Analysis Date = 10/01/13 Pct Recovery = 62% Analysis Date = 10/01/13 Pct Recovery = 62% Analysis Date = 09/21/13 Pct Recovery = 61% Analysis Date = 09/21/13 Pct Recovery = 61% Analysis Date = 09/12/13 Pct Recovery = 62% Analysis Date = 09/12/13 Pct Recovery = 62% Analysis Date = 09/03/13 Pct Recovery = 63% Analysis Date = 09/03/13 Pct Recovery = 63% Analysis Date = 08/25/13 Pct Recovery = 64% Analysis Date = 08/25/13 Pct Recovery = 64% Analysis Date = 08/15/13 Pct Recovery = 66% Analysis Date = 08/15/13 Pct Recovery = 66% Analysis Date = 08/06/13 Pct Recovery = 67% Analysis Date = 08/06/13 Pct Recovery = 67% Analysis Date = 07/28/13 Pct Recovery = 68% Analysis Date = 07/28/13 Pct Recovery = 68% Analysis Date = 07/19/13 Pct Recovery = 69% Analysis Date = 07/19/13 Pct Recovery = 69% Analysis Date = 07/09/13 Pct Recovery = 70% Analysis Date = 07/09/13 Pct Recovery = 70% Analysis Date = 06/30/13 Pct Recovery = 71% Analysis Date = 06/30/13 Pct Recovery = 71% Analysis Date = 06/21/13 Pct Recovery = 72% Analysis Date = 06/21/13 Pct Recovery = 72% Analysis Date = 06/12/13 Pct Recovery = 73% Analysis Date = 06/12/13 Pct Recovery = 73% Analysis Date = 06/02/13 Pct Recovery = 75% Analysis Date = 06/02/13 Pct Recovery = 75% Analysis Date = 05/24/13 Pct Recovery = 76% Analysis Date = 05/24/13 Pct Recovery = 76% Analysis Date = 05/15/13 Pct Recovery = 77% Analysis Date = 05/15/13 Pct Recovery = 77% Analysis Date = 05/06/13 Pct Recovery = 78% Analysis Date = 05/06/13 Pct Recovery = 78% Analysis Date = 04/26/13 Pct Recovery = 79% Analysis Date = 04/26/13 Pct Recovery = 79% Analysis Date = 04/17/13 Pct Recovery = 80% Analysis Date = 04/17/13 Pct Recovery = 80% Analysis Date = 04/08/13 Pct Recovery = 81% Analysis Date = 04/08/13 Pct Recovery = 81% Analysis Date = 03/30/13 Pct Recovery = 81% Analysis Date = 03/30/13 Pct Recovery = 81% Analysis Date = 03/20/13 Pct Recovery = 82% Analysis Date = 03/20/13 Pct Recovery = 82% Analysis Date = 03/11/13 Pct Recovery = 83% Analysis Date = 03/11/13 Pct Recovery = 83% Analysis Date = 03/02/13 Pct Recovery = 83% Analysis Date = 03/02/13 Pct Recovery = 83% Analysis Date = 02/21/13 Pct Recovery = 84% Analysis Date = 02/21/13 Pct Recovery = 84% Analysis Date = 02/11/13 Pct Recovery = 85% Analysis Date = 02/11/13 Pct Recovery = 85% Analysis Date = 02/02/13 Pct Recovery = 86% Analysis Date = 02/02/13 Pct Recovery = 86% Analysis Date = 01/24/13 Pct Recovery = 86% Analysis Date = 01/24/13 Pct Recovery = 86% Analysis Date = 01/15/13 Pct Recovery = 87% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
TERBUFOS-O-ANALOGUE SULFONE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 1 107% . 107% 0%
>= Reporting Level 17 62% 16% 62% 12%
Total 18 65% 19% 63% 17%

Sample Statistics
TERBUFOS-O-ANALOGUE SULFONE

Characteristic N % % Basis
Plotted 18 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 18 .  
False Negatives 0 0% 0 out of 18
Not Spiked 97 .  
False Positives 0 0% 0 out of 97

OBSP Determination:
TERBUTHYLAZINE
METHOD: 2033 , TESTIDCODE: 04022GCM39

Laboratory ID = 20130250061 Lab Value = 0.147 Expected Conc. = 0.15 Report level label = 0.008 Pct Recovery = 98% Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl SpecificMix = A088380 Laboratory ID = 20140100085 Lab Value = 0.141 Expected Conc. = 0.13 Report level label = 0.008 Pct Recovery = 108% Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl SpecificMix = T1130514013 Laboratory ID = 20132490342 Lab Value = 0.140 Expected Conc. = 0.13 Report level label = 0.008 Pct Recovery = 108% Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl SpecificMix = T1130514013 Laboratory ID = 20140230082 Lab Value = 0.078 Expected Conc. = 0.075 Report level label = 0.008 Pct Recovery = 104% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl SpecificMix = A093651 Laboratory ID = 20132420001 Lab Value = 0.082 Expected Conc. = 0.075 Report level label = 0.008 Pct Recovery = 109% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl SpecificMix = A093651 Laboratory ID = 20130810108 Lab Value = 0.079 Expected Conc. = 0.075 Report level label = 0.008 Pct Recovery = 105% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl SpecificMix = T1120530013 Laboratory ID = 20123560092 Lab Value = 0.078 Expected Conc. = 0.075 Report level label = 0.008 Pct Recovery = 105% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = T1120530013 Laboratory ID = 20131370001 Lab Value = 0.080 Expected Conc. = 0.067 Report level label = 0.008 Pct Recovery = 119% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl SpecificMix = 1473000 Laboratory ID = 20140370077 Lab Value = 0.057 Expected Conc. = 0.065 Report level label = 0.008 Pct Recovery = 88% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl SpecificMix = T1130514013 Laboratory ID = 20132690010 Lab Value = 0.083 Expected Conc. = 0.065 Report level label = 0.008 Pct Recovery = 128% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl SpecificMix = T1130514013 Laboratory ID = 20180390003 Lab Value = 0.052 Expected Conc. = 0.053 Report level label = 0.008 Pct Recovery = 97% Analysis Date = 04/06/18 SpikeMix = Spex Organics EN170808006: 100 µl & Abs 071717Pest: 100 µl SpecificMix = 071717Pest Laboratory ID = 20172510330 Lab Value = 0.049 Expected Conc. = 0.053 Report level label = 0.008 Pct Recovery = 93% Analysis Date = 12/29/17 SpikeMix = ChemService 6537100: 100 µl & Abs 071817Pest: 100 µl SpecificMix = 6537100 Laboratory ID = 20163370001 Lab Value = 0.049 Expected Conc. = 0.0517 Report level label = 0.008 Pct Recovery = 95% Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl SpecificMix = B20160331 Laboratory ID = 20163150006 Lab Value = 0.050 Expected Conc. = 0.0517 Report level label = 0.008 Pct Recovery = 96% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl SpecificMix = B20160331 Laboratory ID = 20161880109 Lab Value = 0.052 Expected Conc. = 0.05 Report level label = 0.008 Pct Recovery = 105% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl SpecificMix = 03FF076 Laboratory ID = 20152750006 Lab Value = 0.039 Expected Conc. = 0.048 Report level label = 0.008 Pct Recovery = 81% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl SpecificMix = 040615 Laboratory ID = 20152610011 Lab Value = 0.042 Expected Conc. = 0.048 Report level label = 0.008 Pct Recovery = 88% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl SpecificMix = 040615 Laboratory ID = 20171720140 Lab Value = 0.044 Expected Conc. = 0.0414 Report level label = 0.008 Pct Recovery = 106% Analysis Date = 08/31/17 SpikeMix = Supelco LC20138V: 80 µl & Phenova B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20171660002 Lab Value = 0.047 Expected Conc. = 0.0414 Report level label = 0.008 Pct Recovery = 113% Analysis Date = 08/23/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20170190026 Lab Value = 0.042 Expected Conc. = 0.0414 Report level label = 0.008 Pct Recovery = 100% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20161470001 Lab Value = 0.039 Expected Conc. = 0.0414 Report level label = 0.008 Pct Recovery = 95% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20172020035 Lab Value = 0.041 Expected Conc. = 0.0412 Report level label = 0.008 Pct Recovery = 100% Analysis Date = 11/07/17 SpikeMix = Abs 071717Pest: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20170960001 Lab Value = 0.031 Expected Conc. = 0.04 Report level label = 0.008 Pct Recovery = 78% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl SpecificMix = 03FF076 Laboratory ID = 20142720002 Lab Value = 0.026 Expected Conc. = 0.0318 Report level label = 0.008 Pct Recovery = 81% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl SpecificMix = LC06435 Laboratory ID = 20142530087 Lab Value = 0.026 Expected Conc. = 0.0318 Report level label = 0.008 Pct Recovery = 83% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl SpecificMix = LC06435 Laboratory ID = 20141570088 Lab Value = 0.034 Expected Conc. = 0.0318 Report level label = 0.008 Pct Recovery = 107% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl SpecificMix = LC06435 Laboratory ID = 20141220025 Lab Value = 0.035 Expected Conc. = 0.0318 Report level label = 0.008 Pct Recovery = 110% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl SpecificMix = LC06435 Laboratory ID = 20150720069 Lab Value = 0.031 Expected Conc. = 0.0312 Report level label = 0.008 Pct Recovery = 98% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 03DD006 Laboratory ID = 20143110108 Lab Value = 0.023 Expected Conc. = 0.0312 Report level label = 0.008 Pct Recovery = 72% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 03DD006 Laboratory ID = 20142960086 Lab Value = 0.027 Expected Conc. = 0.0312 Report level label = 0.008 Pct Recovery = 87% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 03DD006 Laboratory ID = 20142270001 Lab Value = 0.024 Expected Conc. = 0.0312 Report level label = 0.008 Pct Recovery = 77% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl SpecificMix = 03DD006 Laboratory ID = 20140860102 Lab Value = 0.026 Expected Conc. = 0.03 Report level label = 0.008 Pct Recovery = 88% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl SpecificMix = A093651 Laboratory ID = 20133400002 Lab Value = 0.034 Expected Conc. = 0.03 Report level label = 0.008 Pct Recovery = 114% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = A093651 Laboratory ID = 20132910008 Lab Value = 0.031 Expected Conc. = 0.03 Report level label = 0.008 Pct Recovery = 105% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = A093651 Laboratory ID = 20131920149 Lab Value = 0.033 Expected Conc. = 0.03 Report level label = 0.008 Pct Recovery = 109% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl SpecificMix = A093651 Laboratory ID = 20131230084 Lab Value = 0.038 Expected Conc. = 0.03 Report level label = 0.008 Pct Recovery = 127% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl SpecificMix = A088380 Laboratory ID = 20130650005 Lab Value = 0.023 Expected Conc. = 0.03 Report level label = 0.008 Pct Recovery = 78% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl SpecificMix = A088380 Laboratory ID = 20130390105 Lab Value = 0.024 Expected Conc. = 0.03 Report level label = 0.008 Pct Recovery = 81% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl SpecificMix = T1120530013 Laboratory ID = 20140730138 Lab Value = 0.027 Expected Conc. = 0.0268 Report level label = 0.008 Pct Recovery = 100% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 1473000 Laboratory ID = 20133470008 Lab Value = 0.029 Expected Conc. = 0.0268 Report level label = 0.008 Pct Recovery = 106% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl SpecificMix = 1473000 Laboratory ID = 20133310030 Lab Value = 0.027 Expected Conc. = 0.0268 Report level label = 0.008 Pct Recovery = 101% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl SpecificMix = 1473000 Laboratory ID = 20131790009 Lab Value = 0.033 Expected Conc. = 0.0268 Report level label = 0.008 Pct Recovery = 122% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl SpecificMix = 1473000 Laboratory ID = 20131650073 Lab Value = 0.035 Expected Conc. = 0.0268 Report level label = 0.008 Pct Recovery = 129% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl SpecificMix = 1473000 Laboratory ID = 20173480003 Lab Value = 0.026 Expected Conc. = 0.0265 Report level label = 0.008 Pct Recovery = 98% Analysis Date = 04/05/18 SpikeMix = Abs 071717Pest: 50 µl & ChemService 6567600: 50 µl SpecificMix = 071717Pest Laboratory ID = 20172370001 Lab Value = 0.023 Expected Conc. = 0.0265 Report level label = 0.008 Pct Recovery = 85% Analysis Date = 11/18/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6537100: 50 µl SpecificMix = 6537100 Laboratory ID = 20172230001 Lab Value = 0.030 Expected Conc. = 0.0265 Report level label = 0.008 Pct Recovery = 114% Analysis Date = 10/19/17 SpikeMix = ChemService 6472100: 50 µl & Abs 071717Pest: 50 µl SpecificMix = 071717Pest Laboratory ID = 20133050050 Lab Value = 0.030 Expected Conc. = 0.026 Report level label = 0.008 Pct Recovery = 116% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl SpecificMix = T1130514013 Laboratory ID = 20132280016 Lab Value = 0.030 Expected Conc. = 0.026 Report level label = 0.008 Pct Recovery = 116% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl SpecificMix = T1130514013 Laboratory ID = 20161260151 Lab Value = 0.020 Expected Conc. = 0.024 Report level label = 0.008 Pct Recovery = 84% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = EN150513008 Laboratory ID = 20160770090 Lab Value = 0.019 Expected Conc. = 0.024 Report level label = 0.008 Pct Recovery = 79% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = EN150513008 Laboratory ID = 20153510109 Lab Value = 0.018 Expected Conc. = 0.024 Report level label = 0.008 Pct Recovery = 75% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = EN150513008 Laboratory ID = 20152330039 Lab Value = 0.020 Expected Conc. = 0.024 Report level label = 0.008 Pct Recovery = 82% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl SpecificMix = EN150513008 Laboratory ID = 20151900132 Lab Value = 0.022 Expected Conc. = 0.024 Report level label = 0.008 Pct Recovery = 91% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl SpecificMix = 040615 Laboratory ID = 20151550293 Lab Value = 0.026 Expected Conc. = 0.024 Report level label = 0.008 Pct Recovery = 109% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl SpecificMix = 040615 Laboratory ID = 20171160110 Lab Value = 0.020 Expected Conc. = 0.0207 Report level label = 0.008 Pct Recovery = 97% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = B20160331 Laboratory ID = 20162380004 Lab Value = 0.020 Expected Conc. = 0.0207 Report level label = 0.008 Pct Recovery = 99% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = B20160331 Laboratory ID = 20162150213 Lab Value = 0.015 Expected Conc. = 0.0207 Report level label = 0.008 Pct Recovery = 74% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl SpecificMix = B20160331 Laboratory ID = 20171510080 Lab Value = 0.020 Expected Conc. = 0.02 Report level label = 0.008 Pct Recovery = 101% Analysis Date = 06/09/17 SpikeMix = Supelco LC20138V: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20170460061 Lab Value = 0.016 Expected Conc. = 0.02 Report level label = 0.008 Pct Recovery = 79% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl SpecificMix = 03FF076 Laboratory ID = 20162660005 Lab Value = 0.015 Expected Conc. = 0.02 Report level label = 0.008 Pct Recovery = 75% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl SpecificMix = 03FF076 Laboratory ID = 20161600087 Lab Value = 0.018 Expected Conc. = 0.02 Report level label = 0.008 Pct Recovery = 88% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20161340228 Lab Value = 0.015 Expected Conc. = 0.02 Report level label = 0.008 Pct Recovery = 77% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl SpecificMix = 03FF076 Laboratory ID = 20161190075 Lab Value = 0.015 Expected Conc. = 0.02 Report level label = 0.008 Pct Recovery = 75% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20180940080 Lab Value = 0.016 Expected Conc. = 0.0159 Report level label = 0.008 Pct Recovery = 101% Analysis Date = 05/31/18 SpikeMix = ChemService 6472100: 30 µl & Abs 071717Pest: 30 µl SpecificMix = 071717Pest Laboratory ID = 20180730064 Lab Value = 0.019 Expected Conc. = 0.0159 Report level label = 0.008 Pct Recovery = 119% Analysis Date = 05/16/18 SpikeMix = Abs 071717Pest: 30 µl & Abs 071817Pest: 30 µl SpecificMix = 071717Pest Laboratory ID = 20173120093 Lab Value = 0.019 Expected Conc. = 0.0159 Report level label = 0.008 Pct Recovery = 119% Analysis Date = 03/10/18 SpikeMix = ChemService 6472100: 30 µl & ChemService 6537100: 30 µl SpecificMix = 6537100 Laboratory ID = 20172780018 Lab Value = 0.013 Expected Conc. = 0.0159 Report level label = 0.008 Pct Recovery = 83% Analysis Date = 02/08/18 SpikeMix = ChemService 6537100: 30 µl & Abs 071817Pest: 30 µl SpecificMix = 6537100 Laboratory ID = 20150150115 Lab Value = 0.012 Expected Conc. = 0.0159 Report level label = 0.008 Pct Recovery = 75% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl SpecificMix = LC06435 Laboratory ID = 20143370094 Lab Value = 0.011 Expected Conc. = 0.0159 Report level label = 0.008 Pct Recovery = 71% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl SpecificMix = LC06435 Laboratory ID = 20141910243 Lab Value = 0.012 Expected Conc. = 0.0159 Report level label = 0.008 Pct Recovery = 76% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = LC06435 Laboratory ID = 20141840097 Lab Value = 0.014 Expected Conc. = 0.0159 Report level label = 0.008 Pct Recovery = 86% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl SpecificMix = LC06435 Laboratory ID = 20142200164 Lab Value = 0.014 Expected Conc. = 0.0156 Report level label = 0.008 Pct Recovery = 92% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 03DD006 Laboratory ID = 20141640076 Lab Value = 0.013 Expected Conc. = 0.0156 Report level label = 0.008 Pct Recovery = 84% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl SpecificMix = 03DD006 Laboratory ID = 20141420140 Lab Value = 0.013 Expected Conc. = 0.0156 Report level label = 0.008 Pct Recovery = 86% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 03DD006 Laboratory ID = 20141080004 Lab Value = 0.014 Expected Conc. = 0.0156 Report level label = 0.008 Pct Recovery = 87% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl SpecificMix = 03DD006 Laboratory ID = 20161050143 Lab Value = 0.011 Expected Conc. = 0.012 Report level label = 0.008 Pct Recovery = 92% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Laboratory ID = 20160430111 Lab Value = 0.013 Expected Conc. = 0.012 Report level label = 0.008 Pct Recovery = 104% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Laboratory ID = 20160560044 Lab Value = 0.010 Expected Conc. = 0.012 Report level label = 0.008 Pct Recovery = 83% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl SpecificMix = EN150513008 Laboratory ID = 20160070059 Lab Value = 0.010 Expected Conc. = 0.012 Report level label = 0.008 Pct Recovery = 86% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = 040615 Laboratory ID = 20153160001 Lab Value = 0.011 Expected Conc. = 0.012 Report level label = 0.008 Pct Recovery = 93% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = EN150513008 Laboratory ID = 20153030068 Lab Value = 0.012 Expected Conc. = 0.012 Report level label = 0.008 Pct Recovery = 97% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150513008 Laboratory ID = 20152190003 Lab Value = 0.010 Expected Conc. = 0.012 Report level label = 0.008 Pct Recovery = 81% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150513008 Laboratory ID = 20151480170 Lab Value = 0.010 Expected Conc. = 0.012 Report level label = 0.008 Pct Recovery = 81% Analysis Date = 06/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150513008 Laboratory ID = 20151380009 Lab Value = 0.010 Expected Conc. = 0.012 Report level label = 0.008 Pct Recovery = 87% Analysis Date = 05/30/15 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Analysis Date = 05/31/18 Pct Recovery = 104% Analysis Date = 05/21/18 Pct Recovery = 103% Analysis Date = 05/21/18 Pct Recovery = 103% Analysis Date = 05/11/18 Pct Recovery = 103% Analysis Date = 05/11/18 Pct Recovery = 103% Analysis Date = 05/01/18 Pct Recovery = 103% Analysis Date = 05/01/18 Pct Recovery = 103% Analysis Date = 04/21/18 Pct Recovery = 103% Analysis Date = 04/21/18 Pct Recovery = 103% Analysis Date = 04/11/18 Pct Recovery = 102% Analysis Date = 04/11/18 Pct Recovery = 102% Analysis Date = 04/02/18 Pct Recovery = 102% Analysis Date = 04/02/18 Pct Recovery = 102% Analysis Date = 03/23/18 Pct Recovery = 102% Analysis Date = 03/23/18 Pct Recovery = 102% Analysis Date = 03/13/18 Pct Recovery = 102% Analysis Date = 03/13/18 Pct Recovery = 102% Analysis Date = 03/03/18 Pct Recovery = 102% Analysis Date = 03/03/18 Pct Recovery = 102% Analysis Date = 02/21/18 Pct Recovery = 101% Analysis Date = 02/21/18 Pct Recovery = 101% Analysis Date = 02/12/18 Pct Recovery = 101% Analysis Date = 02/12/18 Pct Recovery = 101% Analysis Date = 02/02/18 Pct Recovery = 101% Analysis Date = 02/02/18 Pct Recovery = 101% Analysis Date = 01/23/18 Pct Recovery = 101% Analysis Date = 01/23/18 Pct Recovery = 101% Analysis Date = 01/13/18 Pct Recovery = 100% Analysis Date = 01/13/18 Pct Recovery = 100% Analysis Date = 01/03/18 Pct Recovery = 100% Analysis Date = 01/03/18 Pct Recovery = 100% Analysis Date = 12/25/17 Pct Recovery = 100% Analysis Date = 12/25/17 Pct Recovery = 100% Analysis Date = 12/15/17 Pct Recovery = 100% Analysis Date = 12/15/17 Pct Recovery = 100% Analysis Date = 12/05/17 Pct Recovery = 100% Analysis Date = 12/05/17 Pct Recovery = 100% Analysis Date = 11/25/17 Pct Recovery = 99% Analysis Date = 11/25/17 Pct Recovery = 99% Analysis Date = 11/15/17 Pct Recovery = 99% Analysis Date = 11/15/17 Pct Recovery = 99% Analysis Date = 11/05/17 Pct Recovery = 99% Analysis Date = 11/05/17 Pct Recovery = 99% Analysis Date = 10/27/17 Pct Recovery = 99% Analysis Date = 10/27/17 Pct Recovery = 99% Analysis Date = 10/17/17 Pct Recovery = 98% Analysis Date = 10/17/17 Pct Recovery = 98% Analysis Date = 10/07/17 Pct Recovery = 98% Analysis Date = 10/07/17 Pct Recovery = 98% Analysis Date = 09/27/17 Pct Recovery = 98% Analysis Date = 09/27/17 Pct Recovery = 98% Analysis Date = 09/17/17 Pct Recovery = 98% Analysis Date = 09/17/17 Pct Recovery = 98% Analysis Date = 09/08/17 Pct Recovery = 98% Analysis Date = 09/08/17 Pct Recovery = 98% Analysis Date = 08/29/17 Pct Recovery = 97% Analysis Date = 08/29/17 Pct Recovery = 97% Analysis Date = 08/19/17 Pct Recovery = 97% Analysis Date = 08/19/17 Pct Recovery = 97% Analysis Date = 08/09/17 Pct Recovery = 97% Analysis Date = 08/09/17 Pct Recovery = 97% Analysis Date = 07/30/17 Pct Recovery = 97% Analysis Date = 07/30/17 Pct Recovery = 97% Analysis Date = 07/21/17 Pct Recovery = 97% Analysis Date = 07/21/17 Pct Recovery = 97% Analysis Date = 07/11/17 Pct Recovery = 96% Analysis Date = 07/11/17 Pct Recovery = 96% Analysis Date = 07/01/17 Pct Recovery = 96% Analysis Date = 07/01/17 Pct Recovery = 96% Analysis Date = 06/21/17 Pct Recovery = 96% Analysis Date = 06/21/17 Pct Recovery = 96% Analysis Date = 06/11/17 Pct Recovery = 96% Analysis Date = 06/11/17 Pct Recovery = 96% Analysis Date = 06/02/17 Pct Recovery = 96% Analysis Date = 06/02/17 Pct Recovery = 96% Analysis Date = 05/23/17 Pct Recovery = 95% Analysis Date = 05/23/17 Pct Recovery = 95% Analysis Date = 05/13/17 Pct Recovery = 95% Analysis Date = 05/13/17 Pct Recovery = 95% Analysis Date = 05/03/17 Pct Recovery = 95% Analysis Date = 05/03/17 Pct Recovery = 95% Analysis Date = 04/23/17 Pct Recovery = 95% Analysis Date = 04/23/17 Pct Recovery = 95% Analysis Date = 04/13/17 Pct Recovery = 94% Analysis Date = 04/13/17 Pct Recovery = 94% Analysis Date = 04/04/17 Pct Recovery = 94% Analysis Date = 04/04/17 Pct Recovery = 94% Analysis Date = 03/25/17 Pct Recovery = 94% Analysis Date = 03/25/17 Pct Recovery = 94% Analysis Date = 03/15/17 Pct Recovery = 94% Analysis Date = 03/15/17 Pct Recovery = 94% Analysis Date = 03/05/17 Pct Recovery = 94% Analysis Date = 03/05/17 Pct Recovery = 94% Analysis Date = 02/23/17 Pct Recovery = 93% Analysis Date = 02/23/17 Pct Recovery = 93% Analysis Date = 02/14/17 Pct Recovery = 93% Analysis Date = 02/14/17 Pct Recovery = 93% Analysis Date = 02/04/17 Pct Recovery = 93% Analysis Date = 02/04/17 Pct Recovery = 93% Analysis Date = 01/25/17 Pct Recovery = 93% Analysis Date = 01/25/17 Pct Recovery = 93% Analysis Date = 01/15/17 Pct Recovery = 93% Analysis Date = 01/15/17 Pct Recovery = 93% Analysis Date = 01/05/17 Pct Recovery = 92% Analysis Date = 01/05/17 Pct Recovery = 92% Analysis Date = 12/27/16 Pct Recovery = 92% Analysis Date = 12/27/16 Pct Recovery = 92% Analysis Date = 12/17/16 Pct Recovery = 92% Analysis Date = 12/17/16 Pct Recovery = 92% Analysis Date = 12/07/16 Pct Recovery = 92% Analysis Date = 12/07/16 Pct Recovery = 92% Analysis Date = 11/27/16 Pct Recovery = 92% Analysis Date = 11/27/16 Pct Recovery = 92% Analysis Date = 11/17/16 Pct Recovery = 91% Analysis Date = 11/17/16 Pct Recovery = 91% Analysis Date = 11/08/16 Pct Recovery = 91% Analysis Date = 11/08/16 Pct Recovery = 91% Analysis Date = 10/29/16 Pct Recovery = 91% Analysis Date = 10/29/16 Pct Recovery = 91% Analysis Date = 10/19/16 Pct Recovery = 91% Analysis Date = 10/19/16 Pct Recovery = 91% Analysis Date = 10/09/16 Pct Recovery = 91% Analysis Date = 10/09/16 Pct Recovery = 91% Analysis Date = 09/29/16 Pct Recovery = 90% Analysis Date = 09/29/16 Pct Recovery = 90% Analysis Date = 09/19/16 Pct Recovery = 90% Analysis Date = 09/19/16 Pct Recovery = 90% Analysis Date = 09/10/16 Pct Recovery = 90% Analysis Date = 09/10/16 Pct Recovery = 90% Analysis Date = 08/31/16 Pct Recovery = 90% Analysis Date = 08/31/16 Pct Recovery = 90% Analysis Date = 08/21/16 Pct Recovery = 90% Analysis Date = 08/21/16 Pct Recovery = 90% Analysis Date = 08/11/16 Pct Recovery = 90% Analysis Date = 08/11/16 Pct Recovery = 90% Analysis Date = 08/01/16 Pct Recovery = 90% Analysis Date = 08/01/16 Pct Recovery = 90% Analysis Date = 07/23/16 Pct Recovery = 89% Analysis Date = 07/23/16 Pct Recovery = 89% Analysis Date = 07/13/16 Pct Recovery = 89% Analysis Date = 07/13/16 Pct Recovery = 89% Analysis Date = 07/03/16 Pct Recovery = 89% Analysis Date = 07/03/16 Pct Recovery = 89% Analysis Date = 06/23/16 Pct Recovery = 89% Analysis Date = 06/23/16 Pct Recovery = 89% Analysis Date = 06/13/16 Pct Recovery = 89% Analysis Date = 06/13/16 Pct Recovery = 89% Analysis Date = 06/04/16 Pct Recovery = 89% Analysis Date = 06/04/16 Pct Recovery = 89% Analysis Date = 05/25/16 Pct Recovery = 89% Analysis Date = 05/25/16 Pct Recovery = 89% Analysis Date = 05/15/16 Pct Recovery = 88% Analysis Date = 05/15/16 Pct Recovery = 88% Analysis Date = 05/05/16 Pct Recovery = 88% Analysis Date = 05/05/16 Pct Recovery = 88% Analysis Date = 04/25/16 Pct Recovery = 88% Analysis Date = 04/25/16 Pct Recovery = 88% Analysis Date = 04/16/16 Pct Recovery = 88% Analysis Date = 04/16/16 Pct Recovery = 88% Analysis Date = 04/06/16 Pct Recovery = 88% Analysis Date = 04/06/16 Pct Recovery = 88% Analysis Date = 03/27/16 Pct Recovery = 88% Analysis Date = 03/27/16 Pct Recovery = 88% Analysis Date = 03/17/16 Pct Recovery = 88% Analysis Date = 03/17/16 Pct Recovery = 88% Analysis Date = 03/07/16 Pct Recovery = 87% Analysis Date = 03/07/16 Pct Recovery = 87% Analysis Date = 02/26/16 Pct Recovery = 87% Analysis Date = 02/26/16 Pct Recovery = 87% Analysis Date = 02/17/16 Pct Recovery = 87% Analysis Date = 02/17/16 Pct Recovery = 87% Analysis Date = 02/07/16 Pct Recovery = 87% Analysis Date = 02/07/16 Pct Recovery = 87% Analysis Date = 01/28/16 Pct Recovery = 87% Analysis Date = 01/28/16 Pct Recovery = 87% Analysis Date = 01/18/16 Pct Recovery = 87% Analysis Date = 01/18/16 Pct Recovery = 87% Analysis Date = 01/08/16 Pct Recovery = 87% Analysis Date = 01/08/16 Pct Recovery = 87% Analysis Date = 12/30/15 Pct Recovery = 87% Analysis Date = 12/30/15 Pct Recovery = 87% Analysis Date = 12/20/15 Pct Recovery = 87% Analysis Date = 12/20/15 Pct Recovery = 87% Analysis Date = 12/10/15 Pct Recovery = 87% Analysis Date = 12/10/15 Pct Recovery = 87% Analysis Date = 11/30/15 Pct Recovery = 87% Analysis Date = 11/30/15 Pct Recovery = 87% Analysis Date = 11/20/15 Pct Recovery = 87% Analysis Date = 11/20/15 Pct Recovery = 87% Analysis Date = 11/11/15 Pct Recovery = 87% Analysis Date = 11/11/15 Pct Recovery = 87% Analysis Date = 11/01/15 Pct Recovery = 87% Analysis Date = 11/01/15 Pct Recovery = 87% Analysis Date = 10/22/15 Pct Recovery = 87% Analysis Date = 10/22/15 Pct Recovery = 87% Analysis Date = 10/12/15 Pct Recovery = 87% Analysis Date = 10/12/15 Pct Recovery = 87% Analysis Date = 10/02/15 Pct Recovery = 87% Analysis Date = 10/02/15 Pct Recovery = 87% Analysis Date = 09/23/15 Pct Recovery = 87% Analysis Date = 09/23/15 Pct Recovery = 87% Analysis Date = 09/13/15 Pct Recovery = 87% Analysis Date = 09/13/15 Pct Recovery = 87% Analysis Date = 09/03/15 Pct Recovery = 86% Analysis Date = 09/03/15 Pct Recovery = 86% Analysis Date = 08/24/15 Pct Recovery = 86% Analysis Date = 08/24/15 Pct Recovery = 86% Analysis Date = 08/14/15 Pct Recovery = 86% Analysis Date = 08/14/15 Pct Recovery = 86% Analysis Date = 08/04/15 Pct Recovery = 86% Analysis Date = 08/04/15 Pct Recovery = 86% Analysis Date = 07/26/15 Pct Recovery = 86% Analysis Date = 07/26/15 Pct Recovery = 86% Analysis Date = 07/16/15 Pct Recovery = 86% Analysis Date = 07/16/15 Pct Recovery = 86% Analysis Date = 07/06/15 Pct Recovery = 86% Analysis Date = 07/06/15 Pct Recovery = 86% Analysis Date = 06/26/15 Pct Recovery = 86% Analysis Date = 06/26/15 Pct Recovery = 86% Analysis Date = 06/16/15 Pct Recovery = 86% Analysis Date = 06/16/15 Pct Recovery = 86% Analysis Date = 06/07/15 Pct Recovery = 86% Analysis Date = 06/07/15 Pct Recovery = 86% Analysis Date = 05/28/15 Pct Recovery = 86% Analysis Date = 05/28/15 Pct Recovery = 86% Analysis Date = 05/18/15 Pct Recovery = 87% Analysis Date = 05/18/15 Pct Recovery = 87% Analysis Date = 05/08/15 Pct Recovery = 87% Analysis Date = 05/08/15 Pct Recovery = 87% Analysis Date = 04/28/15 Pct Recovery = 87% Analysis Date = 04/28/15 Pct Recovery = 87% Analysis Date = 04/19/15 Pct Recovery = 87% Analysis Date = 04/19/15 Pct Recovery = 87% Analysis Date = 04/09/15 Pct Recovery = 87% Analysis Date = 04/09/15 Pct Recovery = 87% Analysis Date = 03/30/15 Pct Recovery = 87% Analysis Date = 03/30/15 Pct Recovery = 87% Analysis Date = 03/20/15 Pct Recovery = 88% Analysis Date = 03/20/15 Pct Recovery = 88% Analysis Date = 03/10/15 Pct Recovery = 88% Analysis Date = 03/10/15 Pct Recovery = 88% Analysis Date = 02/28/15 Pct Recovery = 88% Analysis Date = 02/28/15 Pct Recovery = 88% Analysis Date = 02/19/15 Pct Recovery = 88% Analysis Date = 02/19/15 Pct Recovery = 88% Analysis Date = 02/09/15 Pct Recovery = 88% Analysis Date = 02/09/15 Pct Recovery = 88% Analysis Date = 01/30/15 Pct Recovery = 88% Analysis Date = 01/30/15 Pct Recovery = 88% Analysis Date = 01/20/15 Pct Recovery = 89% Analysis Date = 01/20/15 Pct Recovery = 89% Analysis Date = 01/10/15 Pct Recovery = 89% Analysis Date = 01/10/15 Pct Recovery = 89% Analysis Date = 01/01/15 Pct Recovery = 89% Analysis Date = 01/01/15 Pct Recovery = 89% Analysis Date = 12/22/14 Pct Recovery = 89% Analysis Date = 12/22/14 Pct Recovery = 89% Analysis Date = 12/12/14 Pct Recovery = 89% Analysis Date = 12/12/14 Pct Recovery = 89% Analysis Date = 12/02/14 Pct Recovery = 89% Analysis Date = 12/02/14 Pct Recovery = 89% Analysis Date = 11/22/14 Pct Recovery = 90% Analysis Date = 11/22/14 Pct Recovery = 90% Analysis Date = 11/13/14 Pct Recovery = 90% Analysis Date = 11/13/14 Pct Recovery = 90% Analysis Date = 11/03/14 Pct Recovery = 90% Analysis Date = 11/03/14 Pct Recovery = 90% Analysis Date = 10/24/14 Pct Recovery = 90% Analysis Date = 10/24/14 Pct Recovery = 90% Analysis Date = 10/14/14 Pct Recovery = 90% Analysis Date = 10/14/14 Pct Recovery = 90% Analysis Date = 10/04/14 Pct Recovery = 90% Analysis Date = 10/04/14 Pct Recovery = 90% Analysis Date = 09/25/14 Pct Recovery = 91% Analysis Date = 09/25/14 Pct Recovery = 91% Analysis Date = 09/15/14 Pct Recovery = 91% Analysis Date = 09/15/14 Pct Recovery = 91% Analysis Date = 09/05/14 Pct Recovery = 91% Analysis Date = 09/05/14 Pct Recovery = 91% Analysis Date = 08/26/14 Pct Recovery = 91% Analysis Date = 08/26/14 Pct Recovery = 91% Analysis Date = 08/16/14 Pct Recovery = 91% Analysis Date = 08/16/14 Pct Recovery = 91% Analysis Date = 08/06/14 Pct Recovery = 92% Analysis Date = 08/06/14 Pct Recovery = 92% Analysis Date = 07/28/14 Pct Recovery = 92% Analysis Date = 07/28/14 Pct Recovery = 92% Analysis Date = 07/18/14 Pct Recovery = 93% Analysis Date = 07/18/14 Pct Recovery = 93% Analysis Date = 07/08/14 Pct Recovery = 93% Analysis Date = 07/08/14 Pct Recovery = 93% Analysis Date = 06/28/14 Pct Recovery = 94% Analysis Date = 06/28/14 Pct Recovery = 94% Analysis Date = 06/18/14 Pct Recovery = 94% Analysis Date = 06/18/14 Pct Recovery = 94% Analysis Date = 06/09/14 Pct Recovery = 94% Analysis Date = 06/09/14 Pct Recovery = 94% Analysis Date = 05/30/14 Pct Recovery = 95% Analysis Date = 05/30/14 Pct Recovery = 95% Analysis Date = 05/20/14 Pct Recovery = 95% Analysis Date = 05/20/14 Pct Recovery = 95% Analysis Date = 05/10/14 Pct Recovery = 96% Analysis Date = 05/10/14 Pct Recovery = 96% Analysis Date = 04/30/14 Pct Recovery = 96% Analysis Date = 04/30/14 Pct Recovery = 96% Analysis Date = 04/21/14 Pct Recovery = 96% Analysis Date = 04/21/14 Pct Recovery = 96% Analysis Date = 04/11/14 Pct Recovery = 97% Analysis Date = 04/11/14 Pct Recovery = 97% Analysis Date = 04/01/14 Pct Recovery = 97% Analysis Date = 04/01/14 Pct Recovery = 97% Analysis Date = 03/22/14 Pct Recovery = 98% Analysis Date = 03/22/14 Pct Recovery = 98% Analysis Date = 03/12/14 Pct Recovery = 98% Analysis Date = 03/12/14 Pct Recovery = 98% Analysis Date = 03/03/14 Pct Recovery = 98% Analysis Date = 03/03/14 Pct Recovery = 98% Analysis Date = 02/21/14 Pct Recovery = 99% Analysis Date = 02/21/14 Pct Recovery = 99% Analysis Date = 02/11/14 Pct Recovery = 99% Analysis Date = 02/11/14 Pct Recovery = 99% Analysis Date = 02/01/14 Pct Recovery = 99% Analysis Date = 02/01/14 Pct Recovery = 99% Analysis Date = 01/22/14 Pct Recovery = 100% Analysis Date = 01/22/14 Pct Recovery = 100% Analysis Date = 01/12/14 Pct Recovery = 100% Analysis Date = 01/12/14 Pct Recovery = 100% Analysis Date = 01/03/14 Pct Recovery = 101% Analysis Date = 01/03/14 Pct Recovery = 101% Analysis Date = 12/24/13 Pct Recovery = 101% Analysis Date = 12/24/13 Pct Recovery = 101% Analysis Date = 12/14/13 Pct Recovery = 101% Analysis Date = 12/14/13 Pct Recovery = 101% Analysis Date = 12/04/13 Pct Recovery = 102% Analysis Date = 12/04/13 Pct Recovery = 102% Analysis Date = 11/24/13 Pct Recovery = 102% Analysis Date = 11/24/13 Pct Recovery = 102% Analysis Date = 11/15/13 Pct Recovery = 102% Analysis Date = 11/15/13 Pct Recovery = 102% Analysis Date = 11/05/13 Pct Recovery = 103% Analysis Date = 11/05/13 Pct Recovery = 103% Analysis Date = 10/26/13 Pct Recovery = 103% Analysis Date = 10/26/13 Pct Recovery = 103% Analysis Date = 10/16/13 Pct Recovery = 103% Analysis Date = 10/16/13 Pct Recovery = 103% Analysis Date = 10/06/13 Pct Recovery = 104% Analysis Date = 10/06/13 Pct Recovery = 104% Analysis Date = 09/27/13 Pct Recovery = 104% Analysis Date = 09/27/13 Pct Recovery = 104% Analysis Date = 09/17/13 Pct Recovery = 104% Analysis Date = 09/17/13 Pct Recovery = 104% Analysis Date = 09/07/13 Pct Recovery = 105% Analysis Date = 09/07/13 Pct Recovery = 105% Analysis Date = 08/28/13 Pct Recovery = 105% Analysis Date = 08/28/13 Pct Recovery = 105% Analysis Date = 08/18/13 Pct Recovery = 106% Analysis Date = 08/18/13 Pct Recovery = 106% Analysis Date = 08/09/13 Pct Recovery = 106% Analysis Date = 08/09/13 Pct Recovery = 106% Analysis Date = 07/30/13 Pct Recovery = 106% Analysis Date = 07/30/13 Pct Recovery = 106% Analysis Date = 07/20/13 Pct Recovery = 107% Analysis Date = 07/20/13 Pct Recovery = 107% Analysis Date = 07/10/13 Pct Recovery = 107% Analysis Date = 07/10/13 Pct Recovery = 107% Analysis Date = 06/30/13 Pct Recovery = 107% Analysis Date = 06/30/13 Pct Recovery = 107% Analysis Date = 06/20/13 Pct Recovery = 108% Analysis Date = 06/20/13 Pct Recovery = 108% Analysis Date = 06/11/13 Pct Recovery = 108% Analysis Date = 06/11/13 Pct Recovery = 108% Analysis Date = 06/01/13 Pct Recovery = 108% Analysis Date = 06/01/13 Pct Recovery = 108% Analysis Date = 05/22/13 Pct Recovery = 109% Analysis Date = 05/22/13 Pct Recovery = 109% Analysis Date = 05/12/13 Pct Recovery = 109% Analysis Date = 05/12/13 Pct Recovery = 109% Analysis Date = 05/02/13 Pct Recovery = 110% Analysis Date = 05/02/13 Pct Recovery = 110% Analysis Date = 04/23/13 Pct Recovery = 110% Analysis Date = 04/23/13 Pct Recovery = 110% Analysis Date = 04/13/13 Pct Recovery = 110% Analysis Date = 04/13/13 Pct Recovery = 110% Analysis Date = 04/03/13 Pct Recovery = 111% Analysis Date = 04/03/13 Pct Recovery = 111% Analysis Date = 03/24/13 Pct Recovery = 111% Analysis Date = 03/24/13 Pct Recovery = 111% Analysis Date = 03/14/13 Pct Recovery = 111% Analysis Date = 03/14/13 Pct Recovery = 111% Analysis Date = 03/05/13 Pct Recovery = 112% Analysis Date = 03/05/13 Pct Recovery = 112% Analysis Date = 02/23/13 Pct Recovery = 112% Analysis Date = 02/23/13 Pct Recovery = 112% Analysis Date = 02/13/13 Pct Recovery = 112% Analysis Date = 02/13/13 Pct Recovery = 112% Analysis Date = 02/03/13 Pct Recovery = 113% Analysis Date = 02/03/13 Pct Recovery = 113% Analysis Date = 01/24/13 Pct Recovery = 113% Analysis Date = 01/24/13 Pct Recovery = 113% Analysis Date = 01/15/13 Pct Recovery = 113% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
TERBUTHYLAZINE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 84 95% 15% 95% 17%
Total 84 95% 15% 95% 17%

Sample Statistics
TERBUTHYLAZINE

Characteristic N % % Basis
Plotted 84 99% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 1 1% Spiked
Spiked 85 .  
False Negatives 0 0% 0 out of 85
Not Spiked 49 .  
False Positives 0 0% 0 out of 49

OBSP Determination:
THIOBENCARB
METHOD: 2033 , TESTIDCODE: 82681GCM35

Laboratory ID = 20132490342 Lab Value = 0.207 Expected Conc. = 0.249 Report level label = 0.016 Pct Recovery = 83% Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20130940097 Lab Value = 0.122 Expected Conc. = 0.152 Report level label = 0.016 Pct Recovery = 80% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = 0507-12-04.2 Laboratory ID = 20123560092 Lab Value = 0.123 Expected Conc. = 0.152 Report level label = 0.016 Pct Recovery = 81% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = 0507-12-04.2 Laboratory ID = 20130810108 Lab Value = 0.113 Expected Conc. = 0.15 Report level label = 0.016 Pct Recovery = 75% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl SpecificMix = LB92783 Laboratory ID = 20130100066 Lab Value = 0.148 Expected Conc. = 0.15 Report level label = 0.016 Pct Recovery = 99% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl SpecificMix = LB92783 Laboratory ID = 20132140002 Lab Value = 0.118 Expected Conc. = 0.125 Report level label = 0.016 Pct Recovery = 94% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl SpecificMix = LB99392 Laboratory ID = 20131370001 Lab Value = 0.137 Expected Conc. = 0.125 Report level label = 0.016 Pct Recovery = 110% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl SpecificMix = LB99392 Laboratory ID = 20140370077 Lab Value = 0.094 Expected Conc. = 0.1245 Report level label = 0.016 Pct Recovery = 75% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20132560001 Lab Value = 0.101 Expected Conc. = 0.1245 Report level label = 0.016 Pct Recovery = 81% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20161880109 Lab Value = 0.107 Expected Conc. = 0.1 Report level label = 0.016 Pct Recovery = 107% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl SpecificMix = 03FF076 Laboratory ID = 20163370001 Lab Value = 0.096 Expected Conc. = 0.0986 Report level label = 0.016 Pct Recovery = 97% Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl SpecificMix = B20160331 Laboratory ID = 20163150006 Lab Value = 0.082 Expected Conc. = 0.0986 Report level label = 0.016 Pct Recovery = 84% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl SpecificMix = B20160331 Laboratory ID = 20152750006 Lab Value = 0.059 Expected Conc. = 0.096 Report level label = 0.016 Pct Recovery = 61% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl SpecificMix = 040615 Laboratory ID = 20152610011 Lab Value = 0.077 Expected Conc. = 0.096 Report level label = 0.016 Pct Recovery = 81% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl SpecificMix = 040615 Laboratory ID = 20170960001 Lab Value = 0.068 Expected Conc. = 0.08 Report level label = 0.016 Pct Recovery = 85% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl SpecificMix = 03FF076 Laboratory ID = 20171720140 Lab Value = 0.088 Expected Conc. = 0.0789 Report level label = 0.016 Pct Recovery = 111% Analysis Date = 08/31/17 SpikeMix = Supelco LC20138V: 80 µl & Phenova B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20171660002 Lab Value = 0.081 Expected Conc. = 0.0789 Report level label = 0.016 Pct Recovery = 103% Analysis Date = 08/23/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20170190026 Lab Value = 0.074 Expected Conc. = 0.0789 Report level label = 0.016 Pct Recovery = 94% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20161470001 Lab Value = 0.081 Expected Conc. = 0.0789 Report level label = 0.016 Pct Recovery = 102% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl SpecificMix = B20160331 Laboratory ID = 20150430092 Lab Value = 0.051 Expected Conc. = 0.0654 Report level label = 0.016 Pct Recovery = 78% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl SpecificMix = 042814 Laboratory ID = 20143240095 Lab Value = 0.066 Expected Conc. = 0.0654 Report level label = 0.016 Pct Recovery = 100% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl SpecificMix = 042814 Laboratory ID = 20142960086 Lab Value = 0.052 Expected Conc. = 0.0654 Report level label = 0.016 Pct Recovery = 80% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 042814 Laboratory ID = 20142530087 Lab Value = 0.049 Expected Conc. = 0.0654 Report level label = 0.016 Pct Recovery = 75% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl SpecificMix = 042814 Laboratory ID = 20150720069 Lab Value = 0.062 Expected Conc. = 0.0642 Report level label = 0.016 Pct Recovery = 96% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 0227-14-08 Laboratory ID = 20141770149 Lab Value = 0.053 Expected Conc. = 0.0642 Report level label = 0.016 Pct Recovery = 82% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl SpecificMix = 0227-14-08 Laboratory ID = 20141570088 Lab Value = 0.061 Expected Conc. = 0.0642 Report level label = 0.016 Pct Recovery = 94% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl SpecificMix = 0227-14-08 Laboratory ID = 20130510051 Lab Value = 0.042 Expected Conc. = 0.0608 Report level label = 0.016 Pct Recovery = 69% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl SpecificMix = 0507-12-04.2 Laboratory ID = 20130390105 Lab Value = 0.033 Expected Conc. = 0.06 Report level label = 0.016 Pct Recovery = 55% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl SpecificMix = LB92783 Laboratory ID = 20172230001 Lab Value = 0.053 Expected Conc. = 0.055 Report level label = 0.016 Pct Recovery = 97% Analysis Date = 10/19/17 SpikeMix = ChemService 6472100: 50 µl & Abs 071717Pest: 50 µl SpecificMix = 6472100 Laboratory ID = 20172560101 Lab Value = 0.045 Expected Conc. = 0.053 Report level label = 0.016 Pct Recovery = 86% Analysis Date = 12/22/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6567600: 50 µl SpecificMix = EN170808006 Laboratory ID = 20172370001 Lab Value = 0.037 Expected Conc. = 0.053 Report level label = 0.016 Pct Recovery = 70% Analysis Date = 11/18/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6537100: 50 µl SpecificMix = EN170808006 Laboratory ID = 20140510043 Lab Value = 0.032 Expected Conc. = 0.05 Report level label = 0.016 Pct Recovery = 64% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl SpecificMix = LB99392 Laboratory ID = 20133470008 Lab Value = 0.049 Expected Conc. = 0.05 Report level label = 0.016 Pct Recovery = 98% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl SpecificMix = LB99392 Laboratory ID = 20133190012 Lab Value = 0.049 Expected Conc. = 0.05 Report level label = 0.016 Pct Recovery = 99% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = LB99392 Laboratory ID = 20133050050 Lab Value = 0.047 Expected Conc. = 0.05 Report level label = 0.016 Pct Recovery = 94% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl SpecificMix = LB99392 Laboratory ID = 20133580036 Lab Value = 0.030 Expected Conc. = 0.0498 Report level label = 0.016 Pct Recovery = 61% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20131790009 Lab Value = 0.025 Expected Conc. = 0.0498 Report level label = 0.016 Pct Recovery = 50% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20131510026 Lab Value = 0.030 Expected Conc. = 0.0498 Report level label = 0.016 Pct Recovery = 60% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl SpecificMix = 0318-13-02.2 Laboratory ID = 20161260151 Lab Value = 0.031 Expected Conc. = 0.048 Report level label = 0.016 Pct Recovery = 65% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = EN150513008 Laboratory ID = 20160770090 Lab Value = 0.030 Expected Conc. = 0.048 Report level label = 0.016 Pct Recovery = 63% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = EN150513008 Laboratory ID = 20153510109 Lab Value = 0.030 Expected Conc. = 0.048 Report level label = 0.016 Pct Recovery = 61% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = EN150513008 Laboratory ID = 20152330039 Lab Value = 0.032 Expected Conc. = 0.048 Report level label = 0.016 Pct Recovery = 66% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl SpecificMix = EN150513008 Laboratory ID = 20151900132 Lab Value = 0.033 Expected Conc. = 0.048 Report level label = 0.016 Pct Recovery = 68% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl SpecificMix = 040615 Laboratory ID = 20151550293 Lab Value = 0.044 Expected Conc. = 0.048 Report level label = 0.016 Pct Recovery = 93% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl SpecificMix = 040615 Laboratory ID = 20172020035 Lab Value = 0.037 Expected Conc. = 0.04 Report level label = 0.016 Pct Recovery = 92% Analysis Date = 11/07/17 SpikeMix = Abs 071717Pest: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20171510080 Lab Value = 0.039 Expected Conc. = 0.04 Report level label = 0.016 Pct Recovery = 98% Analysis Date = 06/09/17 SpikeMix = Supelco LC20138V: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20170460061 Lab Value = 0.034 Expected Conc. = 0.04 Report level label = 0.016 Pct Recovery = 86% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl SpecificMix = 03FF076 Laboratory ID = 20162660005 Lab Value = 0.030 Expected Conc. = 0.04 Report level label = 0.016 Pct Recovery = 74% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl SpecificMix = 03FF076 Laboratory ID = 20161600087 Lab Value = 0.028 Expected Conc. = 0.04 Report level label = 0.016 Pct Recovery = 71% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20161340228 Lab Value = 0.025 Expected Conc. = 0.04 Report level label = 0.016 Pct Recovery = 62% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl SpecificMix = 03FF076 Laboratory ID = 20161190075 Lab Value = 0.022 Expected Conc. = 0.04 Report level label = 0.016 Pct Recovery = 56% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 03FF076 Laboratory ID = 20171160110 Lab Value = 0.035 Expected Conc. = 0.0394 Report level label = 0.016 Pct Recovery = 88% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = B20160331 Laboratory ID = 20162380004 Lab Value = 0.034 Expected Conc. = 0.0394 Report level label = 0.016 Pct Recovery = 86% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = B20160331 Laboratory ID = 20162150213 Lab Value = 0.025 Expected Conc. = 0.0394 Report level label = 0.016 Pct Recovery = 64% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl SpecificMix = B20160331 Laboratory ID = 20173120093 Lab Value = 0.031 Expected Conc. = 0.033 Report level label = 0.016 Pct Recovery = 94% Analysis Date = 03/10/18 SpikeMix = ChemService 6472100: 30 µl & ChemService 6537100: 30 µl SpecificMix = 6472100 Laboratory ID = 20143370094 Lab Value = 0.018 Expected Conc. = 0.0327 Report level label = 0.016 Pct Recovery = 55% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl SpecificMix = 042814 Laboratory ID = 20142820151 Lab Value = 0.027 Expected Conc. = 0.0327 Report level label = 0.016 Pct Recovery = 83% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl SpecificMix = 042814 Laboratory ID = 20142470041 Lab Value = 0.033 Expected Conc. = 0.0327 Report level label = 0.016 Pct Recovery = 100% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl SpecificMix = 042814 Laboratory ID = 20142200164 Lab Value = 0.027 Expected Conc. = 0.0327 Report level label = 0.016 Pct Recovery = 83% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 042814 Laboratory ID = 20141840097 Lab Value = 0.024 Expected Conc. = 0.0321 Report level label = 0.016 Pct Recovery = 74% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20141490205 Lab Value = 0.029 Expected Conc. = 0.0321 Report level label = 0.016 Pct Recovery = 89% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20141420140 Lab Value = 0.032 Expected Conc. = 0.0321 Report level label = 0.016 Pct Recovery = 98% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20141360094 Lab Value = 0.023 Expected Conc. = 0.0321 Report level label = 0.016 Pct Recovery = 73% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20161050143 Lab Value = 0.017 Expected Conc. = 0.024 Report level label = 0.016 Pct Recovery = 70% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Laboratory ID = 20160430111 Lab Value = 0.020 Expected Conc. = 0.024 Report level label = 0.016 Pct Recovery = 82% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Laboratory ID = 20160560044 Lab Value = 0.014 Expected Conc. = 0.024 Report level label = 0.016 Pct Recovery = 60% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl SpecificMix = EN150513008 Laboratory ID = 20160070059 Lab Value = 0.018 Expected Conc. = 0.024 Report level label = 0.016 Pct Recovery = 75% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = 040615 Laboratory ID = 20153160001 Lab Value = 0.017 Expected Conc. = 0.024 Report level label = 0.016 Pct Recovery = 72% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = EN150513008 Laboratory ID = 20153030068 Lab Value = 0.018 Expected Conc. = 0.024 Report level label = 0.016 Pct Recovery = 73% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150513008 Laboratory ID = 20152190003 Lab Value = 0.013 Expected Conc. = 0.024 Report level label = 0.016 Pct Recovery = 53% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150513008 Laboratory ID = 20151480170 Lab Value = 0.016 Expected Conc. = 0.024 Report level label = 0.016 Pct Recovery = 65% Analysis Date = 06/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150513008 Laboratory ID = 20151380009 Lab Value = 0.018 Expected Conc. = 0.024 Report level label = 0.016 Pct Recovery = 75% Analysis Date = 05/30/15 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Laboratory ID = 20151210037 Lab Value = 0.020 Expected Conc. = 0.024 Report level label = 0.016 Pct Recovery = 85% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Analysis Date = 03/10/18 Pct Recovery = 98% Analysis Date = 02/28/18 Pct Recovery = 98% Analysis Date = 02/28/18 Pct Recovery = 98% Analysis Date = 02/19/18 Pct Recovery = 98% Analysis Date = 02/19/18 Pct Recovery = 98% Analysis Date = 02/09/18 Pct Recovery = 97% Analysis Date = 02/09/18 Pct Recovery = 97% Analysis Date = 01/31/18 Pct Recovery = 97% Analysis Date = 01/31/18 Pct Recovery = 97% Analysis Date = 01/22/18 Pct Recovery = 97% Analysis Date = 01/22/18 Pct Recovery = 97% Analysis Date = 01/12/18 Pct Recovery = 96% Analysis Date = 01/12/18 Pct Recovery = 96% Analysis Date = 01/03/18 Pct Recovery = 96% Analysis Date = 01/03/18 Pct Recovery = 96% Analysis Date = 12/24/17 Pct Recovery = 96% Analysis Date = 12/24/17 Pct Recovery = 96% Analysis Date = 12/15/17 Pct Recovery = 95% Analysis Date = 12/15/17 Pct Recovery = 95% Analysis Date = 12/06/17 Pct Recovery = 95% Analysis Date = 12/06/17 Pct Recovery = 95% Analysis Date = 11/26/17 Pct Recovery = 95% Analysis Date = 11/26/17 Pct Recovery = 95% Analysis Date = 11/17/17 Pct Recovery = 94% Analysis Date = 11/17/17 Pct Recovery = 94% Analysis Date = 11/07/17 Pct Recovery = 94% Analysis Date = 11/07/17 Pct Recovery = 94% Analysis Date = 10/29/17 Pct Recovery = 94% Analysis Date = 10/29/17 Pct Recovery = 94% Analysis Date = 10/20/17 Pct Recovery = 93% Analysis Date = 10/20/17 Pct Recovery = 93% Analysis Date = 10/10/17 Pct Recovery = 93% Analysis Date = 10/10/17 Pct Recovery = 93% Analysis Date = 10/01/17 Pct Recovery = 93% Analysis Date = 10/01/17 Pct Recovery = 93% Analysis Date = 09/21/17 Pct Recovery = 92% Analysis Date = 09/21/17 Pct Recovery = 92% Analysis Date = 09/12/17 Pct Recovery = 92% Analysis Date = 09/12/17 Pct Recovery = 92% Analysis Date = 09/03/17 Pct Recovery = 92% Analysis Date = 09/03/17 Pct Recovery = 92% Analysis Date = 08/24/17 Pct Recovery = 91% Analysis Date = 08/24/17 Pct Recovery = 91% Analysis Date = 08/15/17 Pct Recovery = 91% Analysis Date = 08/15/17 Pct Recovery = 91% Analysis Date = 08/05/17 Pct Recovery = 91% Analysis Date = 08/05/17 Pct Recovery = 91% Analysis Date = 07/27/17 Pct Recovery = 90% Analysis Date = 07/27/17 Pct Recovery = 90% Analysis Date = 07/18/17 Pct Recovery = 90% Analysis Date = 07/18/17 Pct Recovery = 90% Analysis Date = 07/08/17 Pct Recovery = 90% Analysis Date = 07/08/17 Pct Recovery = 90% Analysis Date = 06/29/17 Pct Recovery = 89% Analysis Date = 06/29/17 Pct Recovery = 89% Analysis Date = 06/19/17 Pct Recovery = 89% Analysis Date = 06/19/17 Pct Recovery = 89% Analysis Date = 06/10/17 Pct Recovery = 89% Analysis Date = 06/10/17 Pct Recovery = 89% Analysis Date = 06/01/17 Pct Recovery = 88% Analysis Date = 06/01/17 Pct Recovery = 88% Analysis Date = 05/22/17 Pct Recovery = 88% Analysis Date = 05/22/17 Pct Recovery = 88% Analysis Date = 05/13/17 Pct Recovery = 88% Analysis Date = 05/13/17 Pct Recovery = 88% Analysis Date = 05/03/17 Pct Recovery = 87% Analysis Date = 05/03/17 Pct Recovery = 87% Analysis Date = 04/24/17 Pct Recovery = 87% Analysis Date = 04/24/17 Pct Recovery = 87% Analysis Date = 04/15/17 Pct Recovery = 87% Analysis Date = 04/15/17 Pct Recovery = 87% Analysis Date = 04/05/17 Pct Recovery = 86% Analysis Date = 04/05/17 Pct Recovery = 86% Analysis Date = 03/27/17 Pct Recovery = 86% Analysis Date = 03/27/17 Pct Recovery = 86% Analysis Date = 03/17/17 Pct Recovery = 86% Analysis Date = 03/17/17 Pct Recovery = 86% Analysis Date = 03/08/17 Pct Recovery = 85% Analysis Date = 03/08/17 Pct Recovery = 85% Analysis Date = 02/27/17 Pct Recovery = 85% Analysis Date = 02/27/17 Pct Recovery = 85% Analysis Date = 02/17/17 Pct Recovery = 85% Analysis Date = 02/17/17 Pct Recovery = 85% Analysis Date = 02/08/17 Pct Recovery = 84% Analysis Date = 02/08/17 Pct Recovery = 84% Analysis Date = 01/29/17 Pct Recovery = 84% Analysis Date = 01/29/17 Pct Recovery = 84% Analysis Date = 01/20/17 Pct Recovery = 84% Analysis Date = 01/20/17 Pct Recovery = 84% Analysis Date = 01/11/17 Pct Recovery = 83% Analysis Date = 01/11/17 Pct Recovery = 83% Analysis Date = 01/01/17 Pct Recovery = 83% Analysis Date = 01/01/17 Pct Recovery = 83% Analysis Date = 12/23/16 Pct Recovery = 83% Analysis Date = 12/23/16 Pct Recovery = 83% Analysis Date = 12/13/16 Pct Recovery = 82% Analysis Date = 12/13/16 Pct Recovery = 82% Analysis Date = 12/04/16 Pct Recovery = 82% Analysis Date = 12/04/16 Pct Recovery = 82% Analysis Date = 11/25/16 Pct Recovery = 82% Analysis Date = 11/25/16 Pct Recovery = 82% Analysis Date = 11/15/16 Pct Recovery = 81% Analysis Date = 11/15/16 Pct Recovery = 81% Analysis Date = 11/06/16 Pct Recovery = 81% Analysis Date = 11/06/16 Pct Recovery = 81% Analysis Date = 10/27/16 Pct Recovery = 81% Analysis Date = 10/27/16 Pct Recovery = 81% Analysis Date = 10/18/16 Pct Recovery = 80% Analysis Date = 10/18/16 Pct Recovery = 80% Analysis Date = 10/09/16 Pct Recovery = 80% Analysis Date = 10/09/16 Pct Recovery = 80% Analysis Date = 09/29/16 Pct Recovery = 80% Analysis Date = 09/29/16 Pct Recovery = 80% Analysis Date = 09/20/16 Pct Recovery = 79% Analysis Date = 09/20/16 Pct Recovery = 79% Analysis Date = 09/10/16 Pct Recovery = 79% Analysis Date = 09/10/16 Pct Recovery = 79% Analysis Date = 09/01/16 Pct Recovery = 79% Analysis Date = 09/01/16 Pct Recovery = 79% Analysis Date = 08/23/16 Pct Recovery = 79% Analysis Date = 08/23/16 Pct Recovery = 79% Analysis Date = 08/13/16 Pct Recovery = 78% Analysis Date = 08/13/16 Pct Recovery = 78% Analysis Date = 08/04/16 Pct Recovery = 78% Analysis Date = 08/04/16 Pct Recovery = 78% Analysis Date = 07/25/16 Pct Recovery = 78% Analysis Date = 07/25/16 Pct Recovery = 78% Analysis Date = 07/16/16 Pct Recovery = 77% Analysis Date = 07/16/16 Pct Recovery = 77% Analysis Date = 07/07/16 Pct Recovery = 77% Analysis Date = 07/07/16 Pct Recovery = 77% Analysis Date = 06/27/16 Pct Recovery = 77% Analysis Date = 06/27/16 Pct Recovery = 77% Analysis Date = 06/18/16 Pct Recovery = 76% Analysis Date = 06/18/16 Pct Recovery = 76% Analysis Date = 06/08/16 Pct Recovery = 76% Analysis Date = 06/08/16 Pct Recovery = 76% Analysis Date = 05/30/16 Pct Recovery = 76% Analysis Date = 05/30/16 Pct Recovery = 76% Analysis Date = 05/21/16 Pct Recovery = 75% Analysis Date = 05/21/16 Pct Recovery = 75% Analysis Date = 05/11/16 Pct Recovery = 75% Analysis Date = 05/11/16 Pct Recovery = 75% Analysis Date = 05/02/16 Pct Recovery = 75% Analysis Date = 05/02/16 Pct Recovery = 75% Analysis Date = 04/22/16 Pct Recovery = 75% Analysis Date = 04/22/16 Pct Recovery = 75% Analysis Date = 04/13/16 Pct Recovery = 75% Analysis Date = 04/13/16 Pct Recovery = 75% Analysis Date = 04/04/16 Pct Recovery = 75% Analysis Date = 04/04/16 Pct Recovery = 75% Analysis Date = 03/25/16 Pct Recovery = 74% Analysis Date = 03/25/16 Pct Recovery = 74% Analysis Date = 03/16/16 Pct Recovery = 74% Analysis Date = 03/16/16 Pct Recovery = 74% Analysis Date = 03/06/16 Pct Recovery = 74% Analysis Date = 03/06/16 Pct Recovery = 74% Analysis Date = 02/26/16 Pct Recovery = 74% Analysis Date = 02/26/16 Pct Recovery = 74% Analysis Date = 02/17/16 Pct Recovery = 74% Analysis Date = 02/17/16 Pct Recovery = 74% Analysis Date = 02/07/16 Pct Recovery = 74% Analysis Date = 02/07/16 Pct Recovery = 74% Analysis Date = 01/29/16 Pct Recovery = 73% Analysis Date = 01/29/16 Pct Recovery = 73% Analysis Date = 01/19/16 Pct Recovery = 73% Analysis Date = 01/19/16 Pct Recovery = 73% Analysis Date = 01/10/16 Pct Recovery = 73% Analysis Date = 01/10/16 Pct Recovery = 73% Analysis Date = 01/01/16 Pct Recovery = 74% Analysis Date = 01/01/16 Pct Recovery = 74% Analysis Date = 12/22/15 Pct Recovery = 74% Analysis Date = 12/22/15 Pct Recovery = 74% Analysis Date = 12/13/15 Pct Recovery = 74% Analysis Date = 12/13/15 Pct Recovery = 74% Analysis Date = 12/03/15 Pct Recovery = 74% Analysis Date = 12/03/15 Pct Recovery = 74% Analysis Date = 11/24/15 Pct Recovery = 74% Analysis Date = 11/24/15 Pct Recovery = 74% Analysis Date = 11/15/15 Pct Recovery = 74% Analysis Date = 11/15/15 Pct Recovery = 74% Analysis Date = 11/05/15 Pct Recovery = 74% Analysis Date = 11/05/15 Pct Recovery = 74% Analysis Date = 10/27/15 Pct Recovery = 74% Analysis Date = 10/27/15 Pct Recovery = 74% Analysis Date = 10/17/15 Pct Recovery = 74% Analysis Date = 10/17/15 Pct Recovery = 74% Analysis Date = 10/08/15 Pct Recovery = 74% Analysis Date = 10/08/15 Pct Recovery = 74% Analysis Date = 09/29/15 Pct Recovery = 75% Analysis Date = 09/29/15 Pct Recovery = 75% Analysis Date = 09/19/15 Pct Recovery = 75% Analysis Date = 09/19/15 Pct Recovery = 75% Analysis Date = 09/10/15 Pct Recovery = 75% Analysis Date = 09/10/15 Pct Recovery = 75% Analysis Date = 08/31/15 Pct Recovery = 75% Analysis Date = 08/31/15 Pct Recovery = 75% Analysis Date = 08/22/15 Pct Recovery = 75% Analysis Date = 08/22/15 Pct Recovery = 75% Analysis Date = 08/13/15 Pct Recovery = 75% Analysis Date = 08/13/15 Pct Recovery = 75% Analysis Date = 08/03/15 Pct Recovery = 75% Analysis Date = 08/03/15 Pct Recovery = 75% Analysis Date = 07/25/15 Pct Recovery = 75% Analysis Date = 07/25/15 Pct Recovery = 75% Analysis Date = 07/15/15 Pct Recovery = 75% Analysis Date = 07/15/15 Pct Recovery = 75% Analysis Date = 07/06/15 Pct Recovery = 76% Analysis Date = 07/06/15 Pct Recovery = 76% Analysis Date = 06/27/15 Pct Recovery = 76% Analysis Date = 06/27/15 Pct Recovery = 76% Analysis Date = 06/17/15 Pct Recovery = 76% Analysis Date = 06/17/15 Pct Recovery = 76% Analysis Date = 06/08/15 Pct Recovery = 76% Analysis Date = 06/08/15 Pct Recovery = 76% Analysis Date = 05/29/15 Pct Recovery = 76% Analysis Date = 05/29/15 Pct Recovery = 76% Analysis Date = 05/20/15 Pct Recovery = 76% Analysis Date = 05/20/15 Pct Recovery = 76% Analysis Date = 05/11/15 Pct Recovery = 77% Analysis Date = 05/11/15 Pct Recovery = 77% Analysis Date = 05/01/15 Pct Recovery = 77% Analysis Date = 05/01/15 Pct Recovery = 77% Analysis Date = 04/22/15 Pct Recovery = 77% Analysis Date = 04/22/15 Pct Recovery = 77% Analysis Date = 04/12/15 Pct Recovery = 77% Analysis Date = 04/12/15 Pct Recovery = 77% Analysis Date = 04/03/15 Pct Recovery = 77% Analysis Date = 04/03/15 Pct Recovery = 77% Analysis Date = 03/25/15 Pct Recovery = 78% Analysis Date = 03/25/15 Pct Recovery = 78% Analysis Date = 03/15/15 Pct Recovery = 78% Analysis Date = 03/15/15 Pct Recovery = 78% Analysis Date = 03/06/15 Pct Recovery = 78% Analysis Date = 03/06/15 Pct Recovery = 78% Analysis Date = 02/24/15 Pct Recovery = 78% Analysis Date = 02/24/15 Pct Recovery = 78% Analysis Date = 02/15/15 Pct Recovery = 78% Analysis Date = 02/15/15 Pct Recovery = 78% Analysis Date = 02/06/15 Pct Recovery = 79% Analysis Date = 02/06/15 Pct Recovery = 79% Analysis Date = 01/27/15 Pct Recovery = 79% Analysis Date = 01/27/15 Pct Recovery = 79% Analysis Date = 01/18/15 Pct Recovery = 79% Analysis Date = 01/18/15 Pct Recovery = 79% Analysis Date = 01/08/15 Pct Recovery = 79% Analysis Date = 01/08/15 Pct Recovery = 79% Analysis Date = 12/30/14 Pct Recovery = 79% Analysis Date = 12/30/14 Pct Recovery = 79% Analysis Date = 12/21/14 Pct Recovery = 80% Analysis Date = 12/21/14 Pct Recovery = 80% Analysis Date = 12/11/14 Pct Recovery = 80% Analysis Date = 12/11/14 Pct Recovery = 80% Analysis Date = 12/02/14 Pct Recovery = 80% Analysis Date = 12/02/14 Pct Recovery = 80% Analysis Date = 11/22/14 Pct Recovery = 80% Analysis Date = 11/22/14 Pct Recovery = 80% Analysis Date = 11/13/14 Pct Recovery = 80% Analysis Date = 11/13/14 Pct Recovery = 80% Analysis Date = 11/04/14 Pct Recovery = 81% Analysis Date = 11/04/14 Pct Recovery = 81% Analysis Date = 10/25/14 Pct Recovery = 81% Analysis Date = 10/25/14 Pct Recovery = 81% Analysis Date = 10/16/14 Pct Recovery = 81% Analysis Date = 10/16/14 Pct Recovery = 81% Analysis Date = 10/06/14 Pct Recovery = 81% Analysis Date = 10/06/14 Pct Recovery = 81% Analysis Date = 09/27/14 Pct Recovery = 81% Analysis Date = 09/27/14 Pct Recovery = 81% Analysis Date = 09/18/14 Pct Recovery = 81% Analysis Date = 09/18/14 Pct Recovery = 81% Analysis Date = 09/08/14 Pct Recovery = 81% Analysis Date = 09/08/14 Pct Recovery = 81% Analysis Date = 08/30/14 Pct Recovery = 81% Analysis Date = 08/30/14 Pct Recovery = 81% Analysis Date = 08/20/14 Pct Recovery = 82% Analysis Date = 08/20/14 Pct Recovery = 82% Analysis Date = 08/11/14 Pct Recovery = 82% Analysis Date = 08/11/14 Pct Recovery = 82% Analysis Date = 08/02/14 Pct Recovery = 82% Analysis Date = 08/02/14 Pct Recovery = 82% Analysis Date = 07/23/14 Pct Recovery = 82% Analysis Date = 07/23/14 Pct Recovery = 82% Analysis Date = 07/14/14 Pct Recovery = 82% Analysis Date = 07/14/14 Pct Recovery = 82% Analysis Date = 07/04/14 Pct Recovery = 82% Analysis Date = 07/04/14 Pct Recovery = 82% Analysis Date = 06/25/14 Pct Recovery = 82% Analysis Date = 06/25/14 Pct Recovery = 82% Analysis Date = 06/16/14 Pct Recovery = 82% Analysis Date = 06/16/14 Pct Recovery = 82% Analysis Date = 06/06/14 Pct Recovery = 82% Analysis Date = 06/06/14 Pct Recovery = 82% Analysis Date = 05/28/14 Pct Recovery = 82% Analysis Date = 05/28/14 Pct Recovery = 82% Analysis Date = 05/18/14 Pct Recovery = 82% Analysis Date = 05/18/14 Pct Recovery = 82% Analysis Date = 05/09/14 Pct Recovery = 82% Analysis Date = 05/09/14 Pct Recovery = 82% Analysis Date = 04/30/14 Pct Recovery = 82% Analysis Date = 04/30/14 Pct Recovery = 82% Analysis Date = 04/20/14 Pct Recovery = 81% Analysis Date = 04/20/14 Pct Recovery = 81% Analysis Date = 04/11/14 Pct Recovery = 81% Analysis Date = 04/11/14 Pct Recovery = 81% Analysis Date = 04/01/14 Pct Recovery = 81% Analysis Date = 04/01/14 Pct Recovery = 81% Analysis Date = 03/23/14 Pct Recovery = 81% Analysis Date = 03/23/14 Pct Recovery = 81% Analysis Date = 03/14/14 Pct Recovery = 81% Analysis Date = 03/14/14 Pct Recovery = 81% Analysis Date = 03/04/14 Pct Recovery = 81% Analysis Date = 03/04/14 Pct Recovery = 81% Analysis Date = 02/23/14 Pct Recovery = 81% Analysis Date = 02/23/14 Pct Recovery = 81% Analysis Date = 02/13/14 Pct Recovery = 81% Analysis Date = 02/13/14 Pct Recovery = 81% Analysis Date = 02/04/14 Pct Recovery = 81% Analysis Date = 02/04/14 Pct Recovery = 81% Analysis Date = 01/26/14 Pct Recovery = 81% Analysis Date = 01/26/14 Pct Recovery = 81% Analysis Date = 01/16/14 Pct Recovery = 81% Analysis Date = 01/16/14 Pct Recovery = 81% Analysis Date = 01/07/14 Pct Recovery = 81% Analysis Date = 01/07/14 Pct Recovery = 81% Analysis Date = 12/28/13 Pct Recovery = 81% Analysis Date = 12/28/13 Pct Recovery = 81% Analysis Date = 12/19/13 Pct Recovery = 81% Analysis Date = 12/19/13 Pct Recovery = 81% Analysis Date = 12/10/13 Pct Recovery = 81% Analysis Date = 12/10/13 Pct Recovery = 81% Analysis Date = 11/30/13 Pct Recovery = 81% Analysis Date = 11/30/13 Pct Recovery = 81% Analysis Date = 11/21/13 Pct Recovery = 81% Analysis Date = 11/21/13 Pct Recovery = 81% Analysis Date = 11/11/13 Pct Recovery = 81% Analysis Date = 11/11/13 Pct Recovery = 81% Analysis Date = 11/02/13 Pct Recovery = 80% Analysis Date = 11/02/13 Pct Recovery = 80% Analysis Date = 10/24/13 Pct Recovery = 80% Analysis Date = 10/24/13 Pct Recovery = 80% Analysis Date = 10/14/13 Pct Recovery = 80% Analysis Date = 10/14/13 Pct Recovery = 80% Analysis Date = 10/05/13 Pct Recovery = 80% Analysis Date = 10/05/13 Pct Recovery = 80% Analysis Date = 09/25/13 Pct Recovery = 80% Analysis Date = 09/25/13 Pct Recovery = 80% Analysis Date = 09/16/13 Pct Recovery = 80% Analysis Date = 09/16/13 Pct Recovery = 80% Analysis Date = 09/07/13 Pct Recovery = 80% Analysis Date = 09/07/13 Pct Recovery = 80% Analysis Date = 08/28/13 Pct Recovery = 80% Analysis Date = 08/28/13 Pct Recovery = 80% Analysis Date = 08/19/13 Pct Recovery = 80% Analysis Date = 08/19/13 Pct Recovery = 80% Analysis Date = 08/09/13 Pct Recovery = 80% Analysis Date = 08/09/13 Pct Recovery = 80% Analysis Date = 07/31/13 Pct Recovery = 80% Analysis Date = 07/31/13 Pct Recovery = 80% Analysis Date = 07/22/13 Pct Recovery = 80% Analysis Date = 07/22/13 Pct Recovery = 80% Analysis Date = 07/12/13 Pct Recovery = 80% Analysis Date = 07/12/13 Pct Recovery = 80% Analysis Date = 07/03/13 Pct Recovery = 80% Analysis Date = 07/03/13 Pct Recovery = 80% Analysis Date = 06/23/13 Pct Recovery = 80% Analysis Date = 06/23/13 Pct Recovery = 80% Analysis Date = 06/14/13 Pct Recovery = 80% Analysis Date = 06/14/13 Pct Recovery = 80% Analysis Date = 06/05/13 Pct Recovery = 80% Analysis Date = 06/05/13 Pct Recovery = 80% Analysis Date = 05/26/13 Pct Recovery = 79% Analysis Date = 05/26/13 Pct Recovery = 79% Analysis Date = 05/17/13 Pct Recovery = 79% Analysis Date = 05/17/13 Pct Recovery = 79% Analysis Date = 05/07/13 Pct Recovery = 79% Analysis Date = 05/07/13 Pct Recovery = 79% Analysis Date = 04/28/13 Pct Recovery = 79% Analysis Date = 04/28/13 Pct Recovery = 79% Analysis Date = 04/19/13 Pct Recovery = 79% Analysis Date = 04/19/13 Pct Recovery = 79% Analysis Date = 04/09/13 Pct Recovery = 79% Analysis Date = 04/09/13 Pct Recovery = 79% Analysis Date = 03/31/13 Pct Recovery = 79% Analysis Date = 03/31/13 Pct Recovery = 79% Analysis Date = 03/21/13 Pct Recovery = 79% Analysis Date = 03/21/13 Pct Recovery = 79% Analysis Date = 03/12/13 Pct Recovery = 79% Analysis Date = 03/12/13 Pct Recovery = 79% Analysis Date = 03/03/13 Pct Recovery = 79% Analysis Date = 03/03/13 Pct Recovery = 79% Analysis Date = 02/21/13 Pct Recovery = 79% Analysis Date = 02/21/13 Pct Recovery = 79% Analysis Date = 02/12/13 Pct Recovery = 79% Analysis Date = 02/12/13 Pct Recovery = 79% Analysis Date = 02/02/13 Pct Recovery = 79% Analysis Date = 02/02/13 Pct Recovery = 79% Analysis Date = 01/24/13 Pct Recovery = 79% Analysis Date = 01/24/13 Pct Recovery = 79% Analysis Date = 01/15/13 Pct Recovery = 78% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
THIOBENCARB

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 73 80% 15% 81% 19%
Total 73 80% 15% 81% 19%

Sample Statistics
THIOBENCARB

Characteristic N % % Basis
Plotted 73 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 73 .  
False Negatives 0 0% 0 out of 73
Not Spiked 45 .  
False Positives 0 0% 0 out of 45

OBSP Determination:
TRIBUFOS (S,S,S-TRIBUTYLPHOSPHOROTRITHIOATE (DEF))
METHOD: 2033 , TESTIDCODE: 61610GCM39

Laboratory ID = 20140100085 Lab Value = 0.146 Expected Conc. = 0.277 Report level label = 0.018 Pct Recovery = 53% Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl SpecificMix = 042413 Laboratory ID = 20132690010 Lab Value = 0.104 Expected Conc. = 0.1385 Report level label = 0.018 Pct Recovery = 75% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl SpecificMix = 042413 Laboratory ID = 20132560001 Lab Value = 0.087 Expected Conc. = 0.1385 Report level label = 0.018 Pct Recovery = 63% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl SpecificMix = 042413 Laboratory ID = 20132140002 Lab Value = 0.081 Expected Conc. = 0.1355 Report level label = 0.018 Pct Recovery = 60% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl SpecificMix = 04CC101 Laboratory ID = 20130940097 Lab Value = 0.065 Expected Conc. = 0.1255 Report level label = 0.018 Pct Recovery = 52% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = 0507-12-04.2 Laboratory ID = 20123560092 Lab Value = 0.049 Expected Conc. = 0.1255 Report level label = 0.018 Pct Recovery = 39% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = 0507-12-04.2 Laboratory ID = 20130810108 Lab Value = 0.073 Expected Conc. = 0.1251 Report level label = 0.018 Pct Recovery = 58% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl SpecificMix = LB92783 Laboratory ID = 20130100066 Lab Value = 0.063 Expected Conc. = 0.1251 Report level label = 0.018 Pct Recovery = 50% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl SpecificMix = LB92783 Laboratory ID = 20172510330 Lab Value = 0.067 Expected Conc. = 0.122 Report level label = 0.018 Pct Recovery = 55% Analysis Date = 12/29/17 SpikeMix = ChemService 6537100: 100 µl & Abs 071817Pest: 100 µl SpecificMix = 6537100 Laboratory ID = 20162860079 Lab Value = 0.075 Expected Conc. = 0.114 Report level label = 0.018 Pct Recovery = 66% Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl SpecificMix = 060916 Laboratory ID = 20163150006 Lab Value = 0.069 Expected Conc. = 0.114 Report level label = 0.018 Pct Recovery = 61% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl SpecificMix = 060916 Laboratory ID = 20152750006 Lab Value = 0.055 Expected Conc. = 0.1088 Report level label = 0.018 Pct Recovery = 50% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl SpecificMix = 040615 Laboratory ID = 20152610011 Lab Value = 0.065 Expected Conc. = 0.1088 Report level label = 0.018 Pct Recovery = 60% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl SpecificMix = 040615 Laboratory ID = 20171660002 Lab Value = 0.059 Expected Conc. = 0.0912 Report level label = 0.018 Pct Recovery = 65% Analysis Date = 08/23/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = 060916 Laboratory ID = 20170190026 Lab Value = 0.062 Expected Conc. = 0.0912 Report level label = 0.018 Pct Recovery = 68% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl SpecificMix = 060916 Laboratory ID = 20171380001 Lab Value = 0.053 Expected Conc. = 0.0904 Report level label = 0.018 Pct Recovery = 58% Analysis Date = 06/07/17 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 041816 Laboratory ID = 20170740063 Lab Value = 0.063 Expected Conc. = 0.0904 Report level label = 0.018 Pct Recovery = 70% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl SpecificMix = 041816 Laboratory ID = 20161740258 Lab Value = 0.045 Expected Conc. = 0.0904 Report level label = 0.018 Pct Recovery = 50% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 041816 Laboratory ID = 20150720069 Lab Value = 0.056 Expected Conc. = 0.072 Report level label = 0.018 Pct Recovery = 78% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 0227-14-08 Laboratory ID = 20150430092 Lab Value = 0.056 Expected Conc. = 0.072 Report level label = 0.018 Pct Recovery = 78% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl SpecificMix = 042814 Laboratory ID = 20143240095 Lab Value = 0.044 Expected Conc. = 0.072 Report level label = 0.018 Pct Recovery = 61% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl SpecificMix = 042814 Laboratory ID = 20142960086 Lab Value = 0.045 Expected Conc. = 0.072 Report level label = 0.018 Pct Recovery = 62% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 042814 Laboratory ID = 20142530087 Lab Value = 0.042 Expected Conc. = 0.072 Report level label = 0.018 Pct Recovery = 59% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl SpecificMix = 042814 Laboratory ID = 20141770149 Lab Value = 0.049 Expected Conc. = 0.072 Report level label = 0.018 Pct Recovery = 68% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl SpecificMix = 0227-14-08 Laboratory ID = 20141570088 Lab Value = 0.045 Expected Conc. = 0.072 Report level label = 0.018 Pct Recovery = 62% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl SpecificMix = 0227-14-08 Laboratory ID = 20172370001 Lab Value = 0.046 Expected Conc. = 0.061 Report level label = 0.018 Pct Recovery = 75% Analysis Date = 11/18/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6537100: 50 µl SpecificMix = 6537100 Laboratory ID = 20172230001 Lab Value = 0.037 Expected Conc. = 0.06 Report level label = 0.018 Pct Recovery = 62% Analysis Date = 10/19/17 SpikeMix = ChemService 6472100: 50 µl & Abs 071717Pest: 50 µl SpecificMix = 071717Pest Laboratory ID = 20133580036 Lab Value = 0.026 Expected Conc. = 0.0554 Report level label = 0.018 Pct Recovery = 47% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 042413 Laboratory ID = 20133190012 Lab Value = 0.041 Expected Conc. = 0.0554 Report level label = 0.018 Pct Recovery = 74% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 042413 Laboratory ID = 20131650073 Lab Value = 0.037 Expected Conc. = 0.0554 Report level label = 0.018 Pct Recovery = 68% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl SpecificMix = 042413 Laboratory ID = 20151900132 Lab Value = 0.033 Expected Conc. = 0.0544 Report level label = 0.018 Pct Recovery = 61% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl SpecificMix = 040615 Laboratory ID = 20151550293 Lab Value = 0.033 Expected Conc. = 0.0544 Report level label = 0.018 Pct Recovery = 60% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl SpecificMix = 040615 Laboratory ID = 20140730138 Lab Value = 0.031 Expected Conc. = 0.0542 Report level label = 0.018 Pct Recovery = 56% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 04CC101 Laboratory ID = 20140510043 Lab Value = 0.044 Expected Conc. = 0.0542 Report level label = 0.018 Pct Recovery = 81% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 04CC101 Laboratory ID = 20133310030 Lab Value = 0.050 Expected Conc. = 0.0542 Report level label = 0.018 Pct Recovery = 92% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl SpecificMix = 04CC101 Laboratory ID = 20132280016 Lab Value = 0.046 Expected Conc. = 0.0542 Report level label = 0.018 Pct Recovery = 85% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl SpecificMix = 04CC101 Laboratory ID = 20131510026 Lab Value = 0.048 Expected Conc. = 0.0542 Report level label = 0.018 Pct Recovery = 88% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl SpecificMix = 04CC101 Laboratory ID = 20161260151 Lab Value = 0.039 Expected Conc. = 0.054 Report level label = 0.018 Pct Recovery = 71% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = EN150513008 Laboratory ID = 20160770090 Lab Value = 0.034 Expected Conc. = 0.054 Report level label = 0.018 Pct Recovery = 63% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = EN150513008 Laboratory ID = 20153510109 Lab Value = 0.038 Expected Conc. = 0.054 Report level label = 0.018 Pct Recovery = 70% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = EN150513008 Laboratory ID = 20152330039 Lab Value = 0.032 Expected Conc. = 0.054 Report level label = 0.018 Pct Recovery = 60% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl SpecificMix = EN150513008 Laboratory ID = 20130510051 Lab Value = 0.031 Expected Conc. = 0.0502 Report level label = 0.018 Pct Recovery = 61% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl SpecificMix = 0507-12-04.2 Laboratory ID = 20130390105 Lab Value = 0.029 Expected Conc. = 0.05 Report level label = 0.018 Pct Recovery = 58% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl SpecificMix = LB92783 Laboratory ID = 20172020035 Lab Value = 0.039 Expected Conc. = 0.048 Report level label = 0.018 Pct Recovery = 81% Analysis Date = 11/07/17 SpikeMix = Abs 071717Pest: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 071717Pest Laboratory ID = 20171160110 Lab Value = 0.035 Expected Conc. = 0.0456 Report level label = 0.018 Pct Recovery = 78% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = 060916 Laboratory ID = 20162520001 Lab Value = 0.040 Expected Conc. = 0.0456 Report level label = 0.018 Pct Recovery = 87% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl SpecificMix = 060916 Laboratory ID = 20163560019 Lab Value = 0.043 Expected Conc. = 0.0456 Report level label = 0.018 Pct Recovery = 95% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl SpecificMix = 060916 Laboratory ID = 20162380004 Lab Value = 0.036 Expected Conc. = 0.0456 Report level label = 0.018 Pct Recovery = 78% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl SpecificMix = 060916 Laboratory ID = 20171940002 Lab Value = 0.038 Expected Conc. = 0.0452 Report level label = 0.018 Pct Recovery = 84% Analysis Date = 11/10/17 SpikeMix = ChemService 5054800: 40 µl & NSI 041816: 40 µl SpecificMix = 041816 Laboratory ID = 20162020124 Lab Value = 0.031 Expected Conc. = 0.0452 Report level label = 0.018 Pct Recovery = 67% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl SpecificMix = 041816 Laboratory ID = 20161600087 Lab Value = 0.028 Expected Conc. = 0.0452 Report level label = 0.018 Pct Recovery = 61% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 041816 Laboratory ID = 20161340228 Lab Value = 0.030 Expected Conc. = 0.0452 Report level label = 0.018 Pct Recovery = 66% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl SpecificMix = 041816 Laboratory ID = 20161190075 Lab Value = 0.031 Expected Conc. = 0.0452 Report level label = 0.018 Pct Recovery = 68% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl SpecificMix = 041816 Laboratory ID = 20173120093 Lab Value = 0.031 Expected Conc. = 0.0366 Report level label = 0.018 Pct Recovery = 86% Analysis Date = 03/10/18 SpikeMix = ChemService 6472100: 30 µl & ChemService 6537100: 30 µl SpecificMix = 6537100 Laboratory ID = 20172780018 Lab Value = 0.035 Expected Conc. = 0.0366 Report level label = 0.018 Pct Recovery = 96% Analysis Date = 02/08/18 SpikeMix = ChemService 6537100: 30 µl & Abs 071817Pest: 30 µl SpecificMix = 6537100 Laboratory ID = 20143370094 Lab Value = 0.029 Expected Conc. = 0.036 Report level label = 0.018 Pct Recovery = 81% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl SpecificMix = 042814 Laboratory ID = 20142820151 Lab Value = 0.027 Expected Conc. = 0.036 Report level label = 0.018 Pct Recovery = 75% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl SpecificMix = 042814 Laboratory ID = 20142470041 Lab Value = 0.025 Expected Conc. = 0.036 Report level label = 0.018 Pct Recovery = 70% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl SpecificMix = 042814 Laboratory ID = 20142200164 Lab Value = 0.024 Expected Conc. = 0.036 Report level label = 0.018 Pct Recovery = 67% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 042814 Laboratory ID = 20141840097 Lab Value = 0.028 Expected Conc. = 0.036 Report level label = 0.018 Pct Recovery = 77% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20141490205 Lab Value = 0.022 Expected Conc. = 0.036 Report level label = 0.018 Pct Recovery = 62% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20141420140 Lab Value = 0.031 Expected Conc. = 0.036 Report level label = 0.018 Pct Recovery = 85% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20141360094 Lab Value = 0.022 Expected Conc. = 0.036 Report level label = 0.018 Pct Recovery = 61% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20161050143 Lab Value = 0.018 Expected Conc. = 0.0272 Report level label = 0.018 Pct Recovery = 67% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Laboratory ID = 20160430111 Lab Value = 0.020 Expected Conc. = 0.0272 Report level label = 0.018 Pct Recovery = 74% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Laboratory ID = 20160070059 Lab Value = 0.020 Expected Conc. = 0.0272 Report level label = 0.018 Pct Recovery = 74% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = 040615 Laboratory ID = 20151380009 Lab Value = 0.017 Expected Conc. = 0.0272 Report level label = 0.018 Pct Recovery = 63% Analysis Date = 05/30/15 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Laboratory ID = 20151210037 Lab Value = 0.022 Expected Conc. = 0.0272 Report level label = 0.018 Pct Recovery = 80% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Laboratory ID = 20160560044 Lab Value = 0.022 Expected Conc. = 0.027 Report level label = 0.018 Pct Recovery = 80% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl SpecificMix = EN150513008 Laboratory ID = 20153160001 Lab Value = 0.025 Expected Conc. = 0.027 Report level label = 0.018 Pct Recovery = 92% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = EN150513008 Laboratory ID = 20153030068 Lab Value = 0.027 Expected Conc. = 0.027 Report level label = 0.018 Pct Recovery = 99% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150513008 Laboratory ID = 20152190003 Lab Value = 0.017 Expected Conc. = 0.027 Report level label = 0.018 Pct Recovery = 64% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150513008 Laboratory ID = 20151480170 Lab Value = 0.025 Expected Conc. = 0.027 Report level label = 0.018 Pct Recovery = 94% Analysis Date = 06/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150513008 Analysis Date = 03/10/18 Pct Recovery = 76% Analysis Date = 02/28/18 Pct Recovery = 76% Analysis Date = 02/28/18 Pct Recovery = 76% Analysis Date = 02/19/18 Pct Recovery = 76% Analysis Date = 02/19/18 Pct Recovery = 76% Analysis Date = 02/09/18 Pct Recovery = 76% Analysis Date = 02/09/18 Pct Recovery = 76% Analysis Date = 01/31/18 Pct Recovery = 76% Analysis Date = 01/31/18 Pct Recovery = 76% Analysis Date = 01/22/18 Pct Recovery = 76% Analysis Date = 01/22/18 Pct Recovery = 76% Analysis Date = 01/12/18 Pct Recovery = 76% Analysis Date = 01/12/18 Pct Recovery = 76% Analysis Date = 01/03/18 Pct Recovery = 76% Analysis Date = 01/03/18 Pct Recovery = 76% Analysis Date = 12/24/17 Pct Recovery = 75% Analysis Date = 12/24/17 Pct Recovery = 75% Analysis Date = 12/15/17 Pct Recovery = 75% Analysis Date = 12/15/17 Pct Recovery = 75% Analysis Date = 12/06/17 Pct Recovery = 75% Analysis Date = 12/06/17 Pct Recovery = 75% Analysis Date = 11/26/17 Pct Recovery = 75% Analysis Date = 11/26/17 Pct Recovery = 75% Analysis Date = 11/17/17 Pct Recovery = 75% Analysis Date = 11/17/17 Pct Recovery = 75% Analysis Date = 11/07/17 Pct Recovery = 75% Analysis Date = 11/07/17 Pct Recovery = 75% Analysis Date = 10/29/17 Pct Recovery = 75% Analysis Date = 10/29/17 Pct Recovery = 75% Analysis Date = 10/20/17 Pct Recovery = 75% Analysis Date = 10/20/17 Pct Recovery = 75% Analysis Date = 10/10/17 Pct Recovery = 75% Analysis Date = 10/10/17 Pct Recovery = 75% Analysis Date = 10/01/17 Pct Recovery = 75% Analysis Date = 10/01/17 Pct Recovery = 75% Analysis Date = 09/21/17 Pct Recovery = 74% Analysis Date = 09/21/17 Pct Recovery = 74% Analysis Date = 09/12/17 Pct Recovery = 74% Analysis Date = 09/12/17 Pct Recovery = 74% Analysis Date = 09/03/17 Pct Recovery = 74% Analysis Date = 09/03/17 Pct Recovery = 74% Analysis Date = 08/24/17 Pct Recovery = 74% Analysis Date = 08/24/17 Pct Recovery = 74% Analysis Date = 08/15/17 Pct Recovery = 74% Analysis Date = 08/15/17 Pct Recovery = 74% Analysis Date = 08/05/17 Pct Recovery = 74% Analysis Date = 08/05/17 Pct Recovery = 74% Analysis Date = 07/27/17 Pct Recovery = 74% Analysis Date = 07/27/17 Pct Recovery = 74% Analysis Date = 07/18/17 Pct Recovery = 74% Analysis Date = 07/18/17 Pct Recovery = 74% Analysis Date = 07/08/17 Pct Recovery = 74% Analysis Date = 07/08/17 Pct Recovery = 74% Analysis Date = 06/29/17 Pct Recovery = 74% Analysis Date = 06/29/17 Pct Recovery = 74% Analysis Date = 06/19/17 Pct Recovery = 73% Analysis Date = 06/19/17 Pct Recovery = 73% Analysis Date = 06/10/17 Pct Recovery = 73% Analysis Date = 06/10/17 Pct Recovery = 73% Analysis Date = 06/01/17 Pct Recovery = 73% Analysis Date = 06/01/17 Pct Recovery = 73% Analysis Date = 05/22/17 Pct Recovery = 73% Analysis Date = 05/22/17 Pct Recovery = 73% Analysis Date = 05/13/17 Pct Recovery = 73% Analysis Date = 05/13/17 Pct Recovery = 73% Analysis Date = 05/03/17 Pct Recovery = 73% Analysis Date = 05/03/17 Pct Recovery = 73% Analysis Date = 04/24/17 Pct Recovery = 73% Analysis Date = 04/24/17 Pct Recovery = 73% Analysis Date = 04/15/17 Pct Recovery = 73% Analysis Date = 04/15/17 Pct Recovery = 73% Analysis Date = 04/05/17 Pct Recovery = 73% Analysis Date = 04/05/17 Pct Recovery = 73% Analysis Date = 03/27/17 Pct Recovery = 73% Analysis Date = 03/27/17 Pct Recovery = 73% Analysis Date = 03/17/17 Pct Recovery = 72% Analysis Date = 03/17/17 Pct Recovery = 72% Analysis Date = 03/08/17 Pct Recovery = 72% Analysis Date = 03/08/17 Pct Recovery = 72% Analysis Date = 02/27/17 Pct Recovery = 72% Analysis Date = 02/27/17 Pct Recovery = 72% Analysis Date = 02/17/17 Pct Recovery = 72% Analysis Date = 02/17/17 Pct Recovery = 72% Analysis Date = 02/08/17 Pct Recovery = 72% Analysis Date = 02/08/17 Pct Recovery = 72% Analysis Date = 01/29/17 Pct Recovery = 72% Analysis Date = 01/29/17 Pct Recovery = 72% Analysis Date = 01/20/17 Pct Recovery = 72% Analysis Date = 01/20/17 Pct Recovery = 72% Analysis Date = 01/11/17 Pct Recovery = 72% Analysis Date = 01/11/17 Pct Recovery = 72% Analysis Date = 01/01/17 Pct Recovery = 72% Analysis Date = 01/01/17 Pct Recovery = 72% Analysis Date = 12/23/16 Pct Recovery = 72% Analysis Date = 12/23/16 Pct Recovery = 72% Analysis Date = 12/13/16 Pct Recovery = 72% Analysis Date = 12/13/16 Pct Recovery = 72% Analysis Date = 12/04/16 Pct Recovery = 72% Analysis Date = 12/04/16 Pct Recovery = 72% Analysis Date = 11/25/16 Pct Recovery = 71% Analysis Date = 11/25/16 Pct Recovery = 71% Analysis Date = 11/15/16 Pct Recovery = 71% Analysis Date = 11/15/16 Pct Recovery = 71% Analysis Date = 11/06/16 Pct Recovery = 71% Analysis Date = 11/06/16 Pct Recovery = 71% Analysis Date = 10/27/16 Pct Recovery = 71% Analysis Date = 10/27/16 Pct Recovery = 71% Analysis Date = 10/18/16 Pct Recovery = 71% Analysis Date = 10/18/16 Pct Recovery = 71% Analysis Date = 10/09/16 Pct Recovery = 71% Analysis Date = 10/09/16 Pct Recovery = 71% Analysis Date = 09/29/16 Pct Recovery = 71% Analysis Date = 09/29/16 Pct Recovery = 71% Analysis Date = 09/20/16 Pct Recovery = 71% Analysis Date = 09/20/16 Pct Recovery = 71% Analysis Date = 09/10/16 Pct Recovery = 71% Analysis Date = 09/10/16 Pct Recovery = 71% Analysis Date = 09/01/16 Pct Recovery = 71% Analysis Date = 09/01/16 Pct Recovery = 71% Analysis Date = 08/23/16 Pct Recovery = 71% Analysis Date = 08/23/16 Pct Recovery = 71% Analysis Date = 08/13/16 Pct Recovery = 71% Analysis Date = 08/13/16 Pct Recovery = 71% Analysis Date = 08/04/16 Pct Recovery = 71% Analysis Date = 08/04/16 Pct Recovery = 71% Analysis Date = 07/25/16 Pct Recovery = 71% Analysis Date = 07/25/16 Pct Recovery = 71% Analysis Date = 07/16/16 Pct Recovery = 71% Analysis Date = 07/16/16 Pct Recovery = 71% Analysis Date = 07/07/16 Pct Recovery = 71% Analysis Date = 07/07/16 Pct Recovery = 71% Analysis Date = 06/27/16 Pct Recovery = 71% Analysis Date = 06/27/16 Pct Recovery = 71% Analysis Date = 06/18/16 Pct Recovery = 71% Analysis Date = 06/18/16 Pct Recovery = 71% Analysis Date = 06/08/16 Pct Recovery = 70% Analysis Date = 06/08/16 Pct Recovery = 70% Analysis Date = 05/30/16 Pct Recovery = 70% Analysis Date = 05/30/16 Pct Recovery = 70% Analysis Date = 05/21/16 Pct Recovery = 70% Analysis Date = 05/21/16 Pct Recovery = 70% Analysis Date = 05/11/16 Pct Recovery = 70% Analysis Date = 05/11/16 Pct Recovery = 70% Analysis Date = 05/02/16 Pct Recovery = 70% Analysis Date = 05/02/16 Pct Recovery = 70% Analysis Date = 04/22/16 Pct Recovery = 70% Analysis Date = 04/22/16 Pct Recovery = 70% Analysis Date = 04/13/16 Pct Recovery = 70% Analysis Date = 04/13/16 Pct Recovery = 70% Analysis Date = 04/04/16 Pct Recovery = 70% Analysis Date = 04/04/16 Pct Recovery = 70% Analysis Date = 03/25/16 Pct Recovery = 70% Analysis Date = 03/25/16 Pct Recovery = 70% Analysis Date = 03/16/16 Pct Recovery = 70% Analysis Date = 03/16/16 Pct Recovery = 70% Analysis Date = 03/06/16 Pct Recovery = 70% Analysis Date = 03/06/16 Pct Recovery = 70% Analysis Date = 02/26/16 Pct Recovery = 70% Analysis Date = 02/26/16 Pct Recovery = 70% Analysis Date = 02/17/16 Pct Recovery = 70% Analysis Date = 02/17/16 Pct Recovery = 70% Analysis Date = 02/07/16 Pct Recovery = 70% Analysis Date = 02/07/16 Pct Recovery = 70% Analysis Date = 01/29/16 Pct Recovery = 70% Analysis Date = 01/29/16 Pct Recovery = 70% Analysis Date = 01/19/16 Pct Recovery = 70% Analysis Date = 01/19/16 Pct Recovery = 70% Analysis Date = 01/10/16 Pct Recovery = 70% Analysis Date = 01/10/16 Pct Recovery = 70% Analysis Date = 01/01/16 Pct Recovery = 70% Analysis Date = 01/01/16 Pct Recovery = 70% Analysis Date = 12/22/15 Pct Recovery = 70% Analysis Date = 12/22/15 Pct Recovery = 70% Analysis Date = 12/13/15 Pct Recovery = 70% Analysis Date = 12/13/15 Pct Recovery = 70% Analysis Date = 12/03/15 Pct Recovery = 70% Analysis Date = 12/03/15 Pct Recovery = 70% Analysis Date = 11/24/15 Pct Recovery = 70% Analysis Date = 11/24/15 Pct Recovery = 70% Analysis Date = 11/15/15 Pct Recovery = 70% Analysis Date = 11/15/15 Pct Recovery = 70% Analysis Date = 11/05/15 Pct Recovery = 70% Analysis Date = 11/05/15 Pct Recovery = 70% Analysis Date = 10/27/15 Pct Recovery = 70% Analysis Date = 10/27/15 Pct Recovery = 70% Analysis Date = 10/17/15 Pct Recovery = 70% Analysis Date = 10/17/15 Pct Recovery = 70% Analysis Date = 10/08/15 Pct Recovery = 70% Analysis Date = 10/08/15 Pct Recovery = 70% Analysis Date = 09/29/15 Pct Recovery = 70% Analysis Date = 09/29/15 Pct Recovery = 70% Analysis Date = 09/19/15 Pct Recovery = 70% Analysis Date = 09/19/15 Pct Recovery = 70% Analysis Date = 09/10/15 Pct Recovery = 70% Analysis Date = 09/10/15 Pct Recovery = 70% Analysis Date = 08/31/15 Pct Recovery = 70% Analysis Date = 08/31/15 Pct Recovery = 70% Analysis Date = 08/22/15 Pct Recovery = 70% Analysis Date = 08/22/15 Pct Recovery = 70% Analysis Date = 08/13/15 Pct Recovery = 70% Analysis Date = 08/13/15 Pct Recovery = 70% Analysis Date = 08/03/15 Pct Recovery = 70% Analysis Date = 08/03/15 Pct Recovery = 70% Analysis Date = 07/25/15 Pct Recovery = 70% Analysis Date = 07/25/15 Pct Recovery = 70% Analysis Date = 07/15/15 Pct Recovery = 70% Analysis Date = 07/15/15 Pct Recovery = 70% Analysis Date = 07/06/15 Pct Recovery = 70% Analysis Date = 07/06/15 Pct Recovery = 70% Analysis Date = 06/27/15 Pct Recovery = 70% Analysis Date = 06/27/15 Pct Recovery = 70% Analysis Date = 06/17/15 Pct Recovery = 70% Analysis Date = 06/17/15 Pct Recovery = 70% Analysis Date = 06/08/15 Pct Recovery = 70% Analysis Date = 06/08/15 Pct Recovery = 70% Analysis Date = 05/29/15 Pct Recovery = 70% Analysis Date = 05/29/15 Pct Recovery = 70% Analysis Date = 05/20/15 Pct Recovery = 70% Analysis Date = 05/20/15 Pct Recovery = 70% Analysis Date = 05/11/15 Pct Recovery = 70% Analysis Date = 05/11/15 Pct Recovery = 70% Analysis Date = 05/01/15 Pct Recovery = 70% Analysis Date = 05/01/15 Pct Recovery = 70% Analysis Date = 04/22/15 Pct Recovery = 70% Analysis Date = 04/22/15 Pct Recovery = 70% Analysis Date = 04/12/15 Pct Recovery = 70% Analysis Date = 04/12/15 Pct Recovery = 70% Analysis Date = 04/03/15 Pct Recovery = 70% Analysis Date = 04/03/15 Pct Recovery = 70% Analysis Date = 03/25/15 Pct Recovery = 70% Analysis Date = 03/25/15 Pct Recovery = 70% Analysis Date = 03/15/15 Pct Recovery = 70% Analysis Date = 03/15/15 Pct Recovery = 70% Analysis Date = 03/06/15 Pct Recovery = 70% Analysis Date = 03/06/15 Pct Recovery = 70% Analysis Date = 02/24/15 Pct Recovery = 70% Analysis Date = 02/24/15 Pct Recovery = 70% Analysis Date = 02/15/15 Pct Recovery = 70% Analysis Date = 02/15/15 Pct Recovery = 70% Analysis Date = 02/06/15 Pct Recovery = 70% Analysis Date = 02/06/15 Pct Recovery = 70% Analysis Date = 01/27/15 Pct Recovery = 70% Analysis Date = 01/27/15 Pct Recovery = 70% Analysis Date = 01/18/15 Pct Recovery = 70% Analysis Date = 01/18/15 Pct Recovery = 70% Analysis Date = 01/08/15 Pct Recovery = 70% Analysis Date = 01/08/15 Pct Recovery = 70% Analysis Date = 12/30/14 Pct Recovery = 69% Analysis Date = 12/30/14 Pct Recovery = 69% Analysis Date = 12/21/14 Pct Recovery = 69% Analysis Date = 12/21/14 Pct Recovery = 69% Analysis Date = 12/11/14 Pct Recovery = 69% Analysis Date = 12/11/14 Pct Recovery = 69% Analysis Date = 12/02/14 Pct Recovery = 69% Analysis Date = 12/02/14 Pct Recovery = 69% Analysis Date = 11/22/14 Pct Recovery = 69% Analysis Date = 11/22/14 Pct Recovery = 69% Analysis Date = 11/13/14 Pct Recovery = 69% Analysis Date = 11/13/14 Pct Recovery = 69% Analysis Date = 11/04/14 Pct Recovery = 69% Analysis Date = 11/04/14 Pct Recovery = 69% Analysis Date = 10/25/14 Pct Recovery = 69% Analysis Date = 10/25/14 Pct Recovery = 69% Analysis Date = 10/16/14 Pct Recovery = 69% Analysis Date = 10/16/14 Pct Recovery = 69% Analysis Date = 10/06/14 Pct Recovery = 69% Analysis Date = 10/06/14 Pct Recovery = 69% Analysis Date = 09/27/14 Pct Recovery = 69% Analysis Date = 09/27/14 Pct Recovery = 69% Analysis Date = 09/18/14 Pct Recovery = 69% Analysis Date = 09/18/14 Pct Recovery = 69% Analysis Date = 09/08/14 Pct Recovery = 69% Analysis Date = 09/08/14 Pct Recovery = 69% Analysis Date = 08/30/14 Pct Recovery = 69% Analysis Date = 08/30/14 Pct Recovery = 69% Analysis Date = 08/20/14 Pct Recovery = 69% Analysis Date = 08/20/14 Pct Recovery = 69% Analysis Date = 08/11/14 Pct Recovery = 69% Analysis Date = 08/11/14 Pct Recovery = 69% Analysis Date = 08/02/14 Pct Recovery = 69% Analysis Date = 08/02/14 Pct Recovery = 69% Analysis Date = 07/23/14 Pct Recovery = 69% Analysis Date = 07/23/14 Pct Recovery = 69% Analysis Date = 07/14/14 Pct Recovery = 69% Analysis Date = 07/14/14 Pct Recovery = 69% Analysis Date = 07/04/14 Pct Recovery = 69% Analysis Date = 07/04/14 Pct Recovery = 69% Analysis Date = 06/25/14 Pct Recovery = 69% Analysis Date = 06/25/14 Pct Recovery = 69% Analysis Date = 06/16/14 Pct Recovery = 69% Analysis Date = 06/16/14 Pct Recovery = 69% Analysis Date = 06/06/14 Pct Recovery = 69% Analysis Date = 06/06/14 Pct Recovery = 69% Analysis Date = 05/28/14 Pct Recovery = 69% Analysis Date = 05/28/14 Pct Recovery = 69% Analysis Date = 05/18/14 Pct Recovery = 69% Analysis Date = 05/18/14 Pct Recovery = 69% Analysis Date = 05/09/14 Pct Recovery = 68% Analysis Date = 05/09/14 Pct Recovery = 68% Analysis Date = 04/30/14 Pct Recovery = 68% Analysis Date = 04/30/14 Pct Recovery = 68% Analysis Date = 04/20/14 Pct Recovery = 68% Analysis Date = 04/20/14 Pct Recovery = 68% Analysis Date = 04/11/14 Pct Recovery = 68% Analysis Date = 04/11/14 Pct Recovery = 68% Analysis Date = 04/01/14 Pct Recovery = 68% Analysis Date = 04/01/14 Pct Recovery = 68% Analysis Date = 03/23/14 Pct Recovery = 68% Analysis Date = 03/23/14 Pct Recovery = 68% Analysis Date = 03/14/14 Pct Recovery = 67% Analysis Date = 03/14/14 Pct Recovery = 67% Analysis Date = 03/04/14 Pct Recovery = 67% Analysis Date = 03/04/14 Pct Recovery = 67% Analysis Date = 02/23/14 Pct Recovery = 67% Analysis Date = 02/23/14 Pct Recovery = 67% Analysis Date = 02/13/14 Pct Recovery = 67% Analysis Date = 02/13/14 Pct Recovery = 67% Analysis Date = 02/04/14 Pct Recovery = 67% Analysis Date = 02/04/14 Pct Recovery = 67% Analysis Date = 01/26/14 Pct Recovery = 67% Analysis Date = 01/26/14 Pct Recovery = 67% Analysis Date = 01/16/14 Pct Recovery = 67% Analysis Date = 01/16/14 Pct Recovery = 67% Analysis Date = 01/07/14 Pct Recovery = 66% Analysis Date = 01/07/14 Pct Recovery = 66% Analysis Date = 12/28/13 Pct Recovery = 66% Analysis Date = 12/28/13 Pct Recovery = 66% Analysis Date = 12/19/13 Pct Recovery = 66% Analysis Date = 12/19/13 Pct Recovery = 66% Analysis Date = 12/10/13 Pct Recovery = 66% Analysis Date = 12/10/13 Pct Recovery = 66% Analysis Date = 11/30/13 Pct Recovery = 66% Analysis Date = 11/30/13 Pct Recovery = 66% Analysis Date = 11/21/13 Pct Recovery = 65% Analysis Date = 11/21/13 Pct Recovery = 65% Analysis Date = 11/11/13 Pct Recovery = 65% Analysis Date = 11/11/13 Pct Recovery = 65% Analysis Date = 11/02/13 Pct Recovery = 65% Analysis Date = 11/02/13 Pct Recovery = 65% Analysis Date = 10/24/13 Pct Recovery = 65% Analysis Date = 10/24/13 Pct Recovery = 65% Analysis Date = 10/14/13 Pct Recovery = 65% Analysis Date = 10/14/13 Pct Recovery = 65% Analysis Date = 10/05/13 Pct Recovery = 65% Analysis Date = 10/05/13 Pct Recovery = 65% Analysis Date = 09/25/13 Pct Recovery = 64% Analysis Date = 09/25/13 Pct Recovery = 64% Analysis Date = 09/16/13 Pct Recovery = 64% Analysis Date = 09/16/13 Pct Recovery = 64% Analysis Date = 09/07/13 Pct Recovery = 64% Analysis Date = 09/07/13 Pct Recovery = 64% Analysis Date = 08/28/13 Pct Recovery = 64% Analysis Date = 08/28/13 Pct Recovery = 64% Analysis Date = 08/19/13 Pct Recovery = 64% Analysis Date = 08/19/13 Pct Recovery = 64% Analysis Date = 08/09/13 Pct Recovery = 64% Analysis Date = 08/09/13 Pct Recovery = 64% Analysis Date = 07/31/13 Pct Recovery = 63% Analysis Date = 07/31/13 Pct Recovery = 63% Analysis Date = 07/22/13 Pct Recovery = 63% Analysis Date = 07/22/13 Pct Recovery = 63% Analysis Date = 07/12/13 Pct Recovery = 63% Analysis Date = 07/12/13 Pct Recovery = 63% Analysis Date = 07/03/13 Pct Recovery = 63% Analysis Date = 07/03/13 Pct Recovery = 63% Analysis Date = 06/23/13 Pct Recovery = 63% Analysis Date = 06/23/13 Pct Recovery = 63% Analysis Date = 06/14/13 Pct Recovery = 63% Analysis Date = 06/14/13 Pct Recovery = 63% Analysis Date = 06/05/13 Pct Recovery = 62% Analysis Date = 06/05/13 Pct Recovery = 62% Analysis Date = 05/26/13 Pct Recovery = 62% Analysis Date = 05/26/13 Pct Recovery = 62% Analysis Date = 05/17/13 Pct Recovery = 62% Analysis Date = 05/17/13 Pct Recovery = 62% Analysis Date = 05/07/13 Pct Recovery = 62% Analysis Date = 05/07/13 Pct Recovery = 62% Analysis Date = 04/28/13 Pct Recovery = 62% Analysis Date = 04/28/13 Pct Recovery = 62% Analysis Date = 04/19/13 Pct Recovery = 62% Analysis Date = 04/19/13 Pct Recovery = 62% Analysis Date = 04/09/13 Pct Recovery = 61% Analysis Date = 04/09/13 Pct Recovery = 61% Analysis Date = 03/31/13 Pct Recovery = 61% Analysis Date = 03/31/13 Pct Recovery = 61% Analysis Date = 03/21/13 Pct Recovery = 61% Analysis Date = 03/21/13 Pct Recovery = 61% Analysis Date = 03/12/13 Pct Recovery = 61% Analysis Date = 03/12/13 Pct Recovery = 61% Analysis Date = 03/03/13 Pct Recovery = 61% Analysis Date = 03/03/13 Pct Recovery = 61% Analysis Date = 02/21/13 Pct Recovery = 61% Analysis Date = 02/21/13 Pct Recovery = 61% Analysis Date = 02/12/13 Pct Recovery = 60% Analysis Date = 02/12/13 Pct Recovery = 60% Analysis Date = 02/02/13 Pct Recovery = 60% Analysis Date = 02/02/13 Pct Recovery = 60% Analysis Date = 01/24/13 Pct Recovery = 60% Analysis Date = 01/24/13 Pct Recovery = 60% Analysis Date = 01/15/13 Pct Recovery = 60% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
TRIBUFOS (S,S,S-TRIBUTYLPHOSPHOROTRITHIOATE (DEF))

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 73 69% 13% 67% 13%
Total 73 69% 13% 67% 13%

Sample Statistics
TRIBUFOS (S,S,S-TRIBUTYLPHOSPHOROTRITHIOATE (DEF))

Characteristic N % % Basis
Plotted 73 100% Spiked
Estimated Values 73 100% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 73 .  
False Negatives 0 0% 0 out of 73
Not Spiked 45 .  
False Positives 0 0% 0 out of 45

OBSP Determination:
TRIFLURALIN
METHOD: 2033 , TESTIDCODE: 82661GCM35

Laboratory ID = 20140100085 Lab Value = 0.223 Expected Conc. = 0.301 Report level label = 0.018 Pct Recovery = 74% Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl SpecificMix = 042413 Laboratory ID = 20132690010 Lab Value = 0.122 Expected Conc. = 0.1505 Report level label = 0.018 Pct Recovery = 81% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl SpecificMix = 042413 Laboratory ID = 20132560001 Lab Value = 0.108 Expected Conc. = 0.1505 Report level label = 0.018 Pct Recovery = 72% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl SpecificMix = 042413 Laboratory ID = 20132140002 Lab Value = 0.097 Expected Conc. = 0.15 Report level label = 0.018 Pct Recovery = 64% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl SpecificMix = 04CC101 Laboratory ID = 20130250061 Lab Value = 0.093 Expected Conc. = 0.15 Report level label = 0.018 Pct Recovery = 62% Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl SpecificMix = 05BB029 Laboratory ID = 20162860079 Lab Value = 0.087 Expected Conc. = 0.12 Report level label = 0.018 Pct Recovery = 73% Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl SpecificMix = 5054800 Laboratory ID = 20161880109 Lab Value = 0.112 Expected Conc. = 0.12 Report level label = 0.018 Pct Recovery = 93% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl SpecificMix = 5054800 Laboratory ID = 20163370001 Lab Value = 0.090 Expected Conc. = 0.113 Report level label = 0.018 Pct Recovery = 79% Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl SpecificMix = LC20138V Laboratory ID = 20152750006 Lab Value = 0.068 Expected Conc. = 0.108 Report level label = 0.018 Pct Recovery = 63% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl SpecificMix = 040615 Laboratory ID = 20152610011 Lab Value = 0.075 Expected Conc. = 0.108 Report level label = 0.018 Pct Recovery = 69% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl SpecificMix = 040615 Laboratory ID = 20171380001 Lab Value = 0.058 Expected Conc. = 0.096 Report level label = 0.018 Pct Recovery = 60% Analysis Date = 06/07/17 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 5054800 Laboratory ID = 20170960001 Lab Value = 0.067 Expected Conc. = 0.096 Report level label = 0.018 Pct Recovery = 70% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl SpecificMix = 5054800 Laboratory ID = 20161740258 Lab Value = 0.059 Expected Conc. = 0.096 Report level label = 0.018 Pct Recovery = 61% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl SpecificMix = 5054800 Laboratory ID = 20171720140 Lab Value = 0.082 Expected Conc. = 0.0904 Report level label = 0.018 Pct Recovery = 91% Analysis Date = 08/31/17 SpikeMix = Supelco LC20138V: 80 µl & Phenova B20160331: 80 µl SpecificMix = LC20138V Laboratory ID = 20170740063 Lab Value = 0.075 Expected Conc. = 0.0904 Report level label = 0.018 Pct Recovery = 82% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl SpecificMix = LC20138V Laboratory ID = 20161470001 Lab Value = 0.071 Expected Conc. = 0.0904 Report level label = 0.018 Pct Recovery = 78% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl SpecificMix = LC20138V Laboratory ID = 20140230082 Lab Value = 0.053 Expected Conc. = 0.0755 Report level label = 0.018 Pct Recovery = 71% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl SpecificMix = 012513 Laboratory ID = 20132420001 Lab Value = 0.061 Expected Conc. = 0.0755 Report level label = 0.018 Pct Recovery = 81% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl SpecificMix = 012513 Laboratory ID = 20130940097 Lab Value = 0.056 Expected Conc. = 0.0755 Report level label = 0.018 Pct Recovery = 75% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl SpecificMix = 052412 Laboratory ID = 20130100066 Lab Value = 0.067 Expected Conc. = 0.0755 Report level label = 0.018 Pct Recovery = 89% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl SpecificMix = 052412 Laboratory ID = 20150720069 Lab Value = 0.057 Expected Conc. = 0.0726 Report level label = 0.018 Pct Recovery = 79% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 0227-14-08 Laboratory ID = 20141770149 Lab Value = 0.054 Expected Conc. = 0.0726 Report level label = 0.018 Pct Recovery = 74% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl SpecificMix = 0227-14-08 Laboratory ID = 20141570088 Lab Value = 0.059 Expected Conc. = 0.0726 Report level label = 0.018 Pct Recovery = 81% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl SpecificMix = 0227-14-08 Laboratory ID = 20150430092 Lab Value = 0.054 Expected Conc. = 0.072 Report level label = 0.018 Pct Recovery = 75% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl SpecificMix = 042814 Laboratory ID = 20143240095 Lab Value = 0.061 Expected Conc. = 0.072 Report level label = 0.018 Pct Recovery = 85% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl SpecificMix = 042814 Laboratory ID = 20142960086 Lab Value = 0.050 Expected Conc. = 0.072 Report level label = 0.018 Pct Recovery = 70% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl SpecificMix = 042814 Laboratory ID = 20142530087 Lab Value = 0.046 Expected Conc. = 0.072 Report level label = 0.018 Pct Recovery = 63% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl SpecificMix = 042814 Laboratory ID = 20172560101 Lab Value = 0.040 Expected Conc. = 0.061 Report level label = 0.018 Pct Recovery = 65% Analysis Date = 12/22/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6567600: 50 µl SpecificMix = EN170808006 Laboratory ID = 20172370001 Lab Value = 0.051 Expected Conc. = 0.061 Report level label = 0.018 Pct Recovery = 83% Analysis Date = 11/18/17 SpikeMix = Spex Organics EN170808006: 50 µl & ChemService 6537100: 50 µl SpecificMix = EN170808006 Laboratory ID = 20133580036 Lab Value = 0.039 Expected Conc. = 0.0602 Report level label = 0.018 Pct Recovery = 64% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 042413 Laboratory ID = 20133190012 Lab Value = 0.058 Expected Conc. = 0.0602 Report level label = 0.018 Pct Recovery = 96% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 042413 Laboratory ID = 20131650073 Lab Value = 0.055 Expected Conc. = 0.0602 Report level label = 0.018 Pct Recovery = 91% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl SpecificMix = 042413 Laboratory ID = 20172230001 Lab Value = 0.063 Expected Conc. = 0.06 Report level label = 0.018 Pct Recovery = 105% Analysis Date = 10/19/17 SpikeMix = ChemService 6472100: 50 µl & Abs 071717Pest: 50 µl SpecificMix = 6472100 Laboratory ID = 20140730138 Lab Value = 0.044 Expected Conc. = 0.06 Report level label = 0.018 Pct Recovery = 73% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 04CC101 Laboratory ID = 20140510043 Lab Value = 0.051 Expected Conc. = 0.06 Report level label = 0.018 Pct Recovery = 85% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 04CC101 Laboratory ID = 20133310030 Lab Value = 0.057 Expected Conc. = 0.06 Report level label = 0.018 Pct Recovery = 95% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl SpecificMix = 04CC101 Laboratory ID = 20132280016 Lab Value = 0.052 Expected Conc. = 0.06 Report level label = 0.018 Pct Recovery = 86% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl SpecificMix = 04CC101 Laboratory ID = 20131510026 Lab Value = 0.050 Expected Conc. = 0.06 Report level label = 0.018 Pct Recovery = 83% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl SpecificMix = 04CC101 Laboratory ID = 20161260151 Lab Value = 0.043 Expected Conc. = 0.054 Report level label = 0.018 Pct Recovery = 79% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = EN150513008 Laboratory ID = 20160770090 Lab Value = 0.044 Expected Conc. = 0.054 Report level label = 0.018 Pct Recovery = 82% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = EN150513008 Laboratory ID = 20153510109 Lab Value = 0.035 Expected Conc. = 0.054 Report level label = 0.018 Pct Recovery = 64% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl SpecificMix = EN150513008 Laboratory ID = 20152330039 Lab Value = 0.034 Expected Conc. = 0.054 Report level label = 0.018 Pct Recovery = 63% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl SpecificMix = EN150513008 Laboratory ID = 20151900132 Lab Value = 0.050 Expected Conc. = 0.054 Report level label = 0.018 Pct Recovery = 93% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl SpecificMix = 040615 Laboratory ID = 20151550293 Lab Value = 0.043 Expected Conc. = 0.054 Report level label = 0.018 Pct Recovery = 80% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl SpecificMix = 040615 Laboratory ID = 20171940002 Lab Value = 0.042 Expected Conc. = 0.048 Report level label = 0.018 Pct Recovery = 87% Analysis Date = 11/10/17 SpikeMix = ChemService 5054800: 40 µl & NSI 041816: 40 µl SpecificMix = 5054800 Laboratory ID = 20170460061 Lab Value = 0.038 Expected Conc. = 0.048 Report level label = 0.018 Pct Recovery = 78% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl SpecificMix = 5054800 Laboratory ID = 20163560019 Lab Value = 0.042 Expected Conc. = 0.048 Report level label = 0.018 Pct Recovery = 87% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl SpecificMix = 5054800 Laboratory ID = 20162150213 Lab Value = 0.049 Expected Conc. = 0.048 Report level label = 0.018 Pct Recovery = 103% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl SpecificMix = 5054800 Laboratory ID = 20171510080 Lab Value = 0.039 Expected Conc. = 0.0452 Report level label = 0.018 Pct Recovery = 85% Analysis Date = 06/09/17 SpikeMix = Supelco LC20138V: 40 µl & Crescent 03FF076: 40 µl SpecificMix = LC20138V Laboratory ID = 20162520001 Lab Value = 0.048 Expected Conc. = 0.0452 Report level label = 0.018 Pct Recovery = 107% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl SpecificMix = LC20138V Laboratory ID = 20162660005 Lab Value = 0.040 Expected Conc. = 0.0452 Report level label = 0.018 Pct Recovery = 89% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl SpecificMix = LC20138V Laboratory ID = 20162020124 Lab Value = 0.031 Expected Conc. = 0.0452 Report level label = 0.018 Pct Recovery = 69% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl SpecificMix = LC20138V Laboratory ID = 20141840097 Lab Value = 0.029 Expected Conc. = 0.0363 Report level label = 0.018 Pct Recovery = 80% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20141490205 Lab Value = 0.032 Expected Conc. = 0.0363 Report level label = 0.018 Pct Recovery = 88% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20141420140 Lab Value = 0.026 Expected Conc. = 0.0363 Report level label = 0.018 Pct Recovery = 71% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20141360094 Lab Value = 0.029 Expected Conc. = 0.0363 Report level label = 0.018 Pct Recovery = 80% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl SpecificMix = 0227-14-08 Laboratory ID = 20173120093 Lab Value = 0.039 Expected Conc. = 0.036 Report level label = 0.018 Pct Recovery = 108% Analysis Date = 03/10/18 SpikeMix = ChemService 6472100: 30 µl & ChemService 6537100: 30 µl SpecificMix = 6472100 Laboratory ID = 20143370094 Lab Value = 0.029 Expected Conc. = 0.036 Report level label = 0.018 Pct Recovery = 81% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl SpecificMix = 042814 Laboratory ID = 20142820151 Lab Value = 0.030 Expected Conc. = 0.036 Report level label = 0.018 Pct Recovery = 83% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl SpecificMix = 042814 Laboratory ID = 20142470041 Lab Value = 0.030 Expected Conc. = 0.036 Report level label = 0.018 Pct Recovery = 83% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl SpecificMix = 042814 Laboratory ID = 20142200164 Lab Value = 0.030 Expected Conc. = 0.036 Report level label = 0.018 Pct Recovery = 83% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl SpecificMix = 042814 Laboratory ID = 20140860102 Lab Value = 0.023 Expected Conc. = 0.0302 Report level label = 0.018 Pct Recovery = 77% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl SpecificMix = 012513 Laboratory ID = 20133400002 Lab Value = 0.026 Expected Conc. = 0.0302 Report level label = 0.018 Pct Recovery = 86% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = 052412 Laboratory ID = 20132910008 Lab Value = 0.028 Expected Conc. = 0.0302 Report level label = 0.018 Pct Recovery = 92% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl SpecificMix = 052412 Laboratory ID = 20131920149 Lab Value = 0.028 Expected Conc. = 0.0302 Report level label = 0.018 Pct Recovery = 92% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl SpecificMix = 012513 Laboratory ID = 20130650005 Lab Value = 0.020 Expected Conc. = 0.0302 Report level label = 0.018 Pct Recovery = 67% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl SpecificMix = 052412 Laboratory ID = 20131230084 Lab Value = 0.027 Expected Conc. = 0.03 Report level label = 0.018 Pct Recovery = 90% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl SpecificMix = 05BB029 Laboratory ID = 20130510051 Lab Value = 0.030 Expected Conc. = 0.03 Report level label = 0.018 Pct Recovery = 100% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl SpecificMix = 05BB029 Laboratory ID = 20161050143 Lab Value = 0.024 Expected Conc. = 0.027 Report level label = 0.018 Pct Recovery = 89% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Laboratory ID = 20160430111 Lab Value = 0.027 Expected Conc. = 0.027 Report level label = 0.018 Pct Recovery = 99% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Laboratory ID = 20160560044 Lab Value = 0.025 Expected Conc. = 0.027 Report level label = 0.018 Pct Recovery = 92% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl SpecificMix = EN150513008 Laboratory ID = 20160070059 Lab Value = 0.019 Expected Conc. = 0.027 Report level label = 0.018 Pct Recovery = 69% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = 040615 Laboratory ID = 20153160001 Lab Value = 0.021 Expected Conc. = 0.027 Report level label = 0.018 Pct Recovery = 79% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl SpecificMix = EN150513008 Laboratory ID = 20153030068 Lab Value = 0.023 Expected Conc. = 0.027 Report level label = 0.018 Pct Recovery = 84% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150513008 Laboratory ID = 20152190003 Lab Value = 0.017 Expected Conc. = 0.027 Report level label = 0.018 Pct Recovery = 62% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150513008 Laboratory ID = 20151480170 Lab Value = 0.026 Expected Conc. = 0.027 Report level label = 0.018 Pct Recovery = 97% Analysis Date = 06/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & Spex Organics EN150513008: 20 µl SpecificMix = EN150513008 Laboratory ID = 20151380009 Lab Value = 0.020 Expected Conc. = 0.027 Report level label = 0.018 Pct Recovery = 75% Analysis Date = 05/30/15 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Laboratory ID = 20151210037 Lab Value = 0.021 Expected Conc. = 0.027 Report level label = 0.018 Pct Recovery = 79% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl SpecificMix = 040615 Analysis Date = 03/09/18 Pct Recovery = 88% Analysis Date = 02/28/18 Pct Recovery = 88% Analysis Date = 02/28/18 Pct Recovery = 88% Analysis Date = 02/19/18 Pct Recovery = 88% Analysis Date = 02/19/18 Pct Recovery = 88% Analysis Date = 02/09/18 Pct Recovery = 88% Analysis Date = 02/09/18 Pct Recovery = 88% Analysis Date = 01/31/18 Pct Recovery = 88% Analysis Date = 01/31/18 Pct Recovery = 88% Analysis Date = 01/22/18 Pct Recovery = 88% Analysis Date = 01/22/18 Pct Recovery = 88% Analysis Date = 01/12/18 Pct Recovery = 88% Analysis Date = 01/12/18 Pct Recovery = 88% Analysis Date = 01/03/18 Pct Recovery = 87% Analysis Date = 01/03/18 Pct Recovery = 87% Analysis Date = 12/24/17 Pct Recovery = 87% Analysis Date = 12/24/17 Pct Recovery = 87% Analysis Date = 12/15/17 Pct Recovery = 87% Analysis Date = 12/15/17 Pct Recovery = 87% Analysis Date = 12/06/17 Pct Recovery = 87% Analysis Date = 12/06/17 Pct Recovery = 87% Analysis Date = 11/26/17 Pct Recovery = 87% Analysis Date = 11/26/17 Pct Recovery = 87% Analysis Date = 11/17/17 Pct Recovery = 87% Analysis Date = 11/17/17 Pct Recovery = 87% Analysis Date = 11/07/17 Pct Recovery = 87% Analysis Date = 11/07/17 Pct Recovery = 87% Analysis Date = 10/29/17 Pct Recovery = 87% Analysis Date = 10/29/17 Pct Recovery = 87% Analysis Date = 10/20/17 Pct Recovery = 86% Analysis Date = 10/20/17 Pct Recovery = 86% Analysis Date = 10/10/17 Pct Recovery = 86% Analysis Date = 10/10/17 Pct Recovery = 86% Analysis Date = 10/01/17 Pct Recovery = 86% Analysis Date = 10/01/17 Pct Recovery = 86% Analysis Date = 09/21/17 Pct Recovery = 86% Analysis Date = 09/21/17 Pct Recovery = 86% Analysis Date = 09/12/17 Pct Recovery = 86% Analysis Date = 09/12/17 Pct Recovery = 86% Analysis Date = 09/03/17 Pct Recovery = 86% Analysis Date = 09/03/17 Pct Recovery = 86% Analysis Date = 08/24/17 Pct Recovery = 86% Analysis Date = 08/24/17 Pct Recovery = 86% Analysis Date = 08/15/17 Pct Recovery = 86% Analysis Date = 08/15/17 Pct Recovery = 86% Analysis Date = 08/06/17 Pct Recovery = 85% Analysis Date = 08/06/17 Pct Recovery = 85% Analysis Date = 07/27/17 Pct Recovery = 85% Analysis Date = 07/27/17 Pct Recovery = 85% Analysis Date = 07/18/17 Pct Recovery = 85% Analysis Date = 07/18/17 Pct Recovery = 85% Analysis Date = 07/08/17 Pct Recovery = 85% Analysis Date = 07/08/17 Pct Recovery = 85% Analysis Date = 06/29/17 Pct Recovery = 85% Analysis Date = 06/29/17 Pct Recovery = 85% Analysis Date = 06/20/17 Pct Recovery = 85% Analysis Date = 06/20/17 Pct Recovery = 85% Analysis Date = 06/10/17 Pct Recovery = 85% Analysis Date = 06/10/17 Pct Recovery = 85% Analysis Date = 06/01/17 Pct Recovery = 85% Analysis Date = 06/01/17 Pct Recovery = 85% Analysis Date = 05/22/17 Pct Recovery = 84% Analysis Date = 05/22/17 Pct Recovery = 84% Analysis Date = 05/13/17 Pct Recovery = 84% Analysis Date = 05/13/17 Pct Recovery = 84% Analysis Date = 05/04/17 Pct Recovery = 84% Analysis Date = 05/04/17 Pct Recovery = 84% Analysis Date = 04/24/17 Pct Recovery = 84% Analysis Date = 04/24/17 Pct Recovery = 84% Analysis Date = 04/15/17 Pct Recovery = 84% Analysis Date = 04/15/17 Pct Recovery = 84% Analysis Date = 04/05/17 Pct Recovery = 84% Analysis Date = 04/05/17 Pct Recovery = 84% Analysis Date = 03/27/17 Pct Recovery = 84% Analysis Date = 03/27/17 Pct Recovery = 84% Analysis Date = 03/18/17 Pct Recovery = 84% Analysis Date = 03/18/17 Pct Recovery = 84% Analysis Date = 03/08/17 Pct Recovery = 83% Analysis Date = 03/08/17 Pct Recovery = 83% Analysis Date = 02/27/17 Pct Recovery = 83% Analysis Date = 02/27/17 Pct Recovery = 83% Analysis Date = 02/18/17 Pct Recovery = 83% Analysis Date = 02/18/17 Pct Recovery = 83% Analysis Date = 02/08/17 Pct Recovery = 83% Analysis Date = 02/08/17 Pct Recovery = 83% Analysis Date = 01/30/17 Pct Recovery = 83% Analysis Date = 01/30/17 Pct Recovery = 83% Analysis Date = 01/20/17 Pct Recovery = 83% Analysis Date = 01/20/17 Pct Recovery = 83% Analysis Date = 01/11/17 Pct Recovery = 83% Analysis Date = 01/11/17 Pct Recovery = 83% Analysis Date = 01/02/17 Pct Recovery = 83% Analysis Date = 01/02/17 Pct Recovery = 83% Analysis Date = 12/23/16 Pct Recovery = 82% Analysis Date = 12/23/16 Pct Recovery = 82% Analysis Date = 12/14/16 Pct Recovery = 82% Analysis Date = 12/14/16 Pct Recovery = 82% Analysis Date = 12/04/16 Pct Recovery = 82% Analysis Date = 12/04/16 Pct Recovery = 82% Analysis Date = 11/25/16 Pct Recovery = 82% Analysis Date = 11/25/16 Pct Recovery = 82% Analysis Date = 11/16/16 Pct Recovery = 82% Analysis Date = 11/16/16 Pct Recovery = 82% Analysis Date = 11/06/16 Pct Recovery = 82% Analysis Date = 11/06/16 Pct Recovery = 82% Analysis Date = 10/28/16 Pct Recovery = 82% Analysis Date = 10/28/16 Pct Recovery = 82% Analysis Date = 10/18/16 Pct Recovery = 82% Analysis Date = 10/18/16 Pct Recovery = 82% Analysis Date = 10/09/16 Pct Recovery = 81% Analysis Date = 10/09/16 Pct Recovery = 81% Analysis Date = 09/30/16 Pct Recovery = 81% Analysis Date = 09/30/16 Pct Recovery = 81% Analysis Date = 09/20/16 Pct Recovery = 81% Analysis Date = 09/20/16 Pct Recovery = 81% Analysis Date = 09/11/16 Pct Recovery = 81% Analysis Date = 09/11/16 Pct Recovery = 81% Analysis Date = 09/01/16 Pct Recovery = 81% Analysis Date = 09/01/16 Pct Recovery = 81% Analysis Date = 08/23/16 Pct Recovery = 81% Analysis Date = 08/23/16 Pct Recovery = 81% Analysis Date = 08/14/16 Pct Recovery = 81% Analysis Date = 08/14/16 Pct Recovery = 81% Analysis Date = 08/04/16 Pct Recovery = 81% Analysis Date = 08/04/16 Pct Recovery = 81% Analysis Date = 07/26/16 Pct Recovery = 81% Analysis Date = 07/26/16 Pct Recovery = 81% Analysis Date = 07/17/16 Pct Recovery = 81% Analysis Date = 07/17/16 Pct Recovery = 81% Analysis Date = 07/07/16 Pct Recovery = 80% Analysis Date = 07/07/16 Pct Recovery = 80% Analysis Date = 06/28/16 Pct Recovery = 80% Analysis Date = 06/28/16 Pct Recovery = 80% Analysis Date = 06/18/16 Pct Recovery = 80% Analysis Date = 06/18/16 Pct Recovery = 80% Analysis Date = 06/09/16 Pct Recovery = 80% Analysis Date = 06/09/16 Pct Recovery = 80% Analysis Date = 05/31/16 Pct Recovery = 80% Analysis Date = 05/31/16 Pct Recovery = 80% Analysis Date = 05/21/16 Pct Recovery = 80% Analysis Date = 05/21/16 Pct Recovery = 80% Analysis Date = 05/12/16 Pct Recovery = 80% Analysis Date = 05/12/16 Pct Recovery = 80% Analysis Date = 05/02/16 Pct Recovery = 80% Analysis Date = 05/02/16 Pct Recovery = 80% Analysis Date = 04/23/16 Pct Recovery = 80% Analysis Date = 04/23/16 Pct Recovery = 80% Analysis Date = 04/14/16 Pct Recovery = 80% Analysis Date = 04/14/16 Pct Recovery = 80% Analysis Date = 04/04/16 Pct Recovery = 80% Analysis Date = 04/04/16 Pct Recovery = 80% Analysis Date = 03/26/16 Pct Recovery = 80% Analysis Date = 03/26/16 Pct Recovery = 80% Analysis Date = 03/16/16 Pct Recovery = 80% Analysis Date = 03/16/16 Pct Recovery = 80% Analysis Date = 03/07/16 Pct Recovery = 80% Analysis Date = 03/07/16 Pct Recovery = 80% Analysis Date = 02/27/16 Pct Recovery = 79% Analysis Date = 02/27/16 Pct Recovery = 79% Analysis Date = 02/17/16 Pct Recovery = 79% Analysis Date = 02/17/16 Pct Recovery = 79% Analysis Date = 02/08/16 Pct Recovery = 79% Analysis Date = 02/08/16 Pct Recovery = 79% Analysis Date = 01/30/16 Pct Recovery = 79% Analysis Date = 01/30/16 Pct Recovery = 79% Analysis Date = 01/20/16 Pct Recovery = 79% Analysis Date = 01/20/16 Pct Recovery = 79% Analysis Date = 01/11/16 Pct Recovery = 79% Analysis Date = 01/11/16 Pct Recovery = 79% Analysis Date = 01/01/16 Pct Recovery = 79% Analysis Date = 01/01/16 Pct Recovery = 79% Analysis Date = 12/23/15 Pct Recovery = 79% Analysis Date = 12/23/15 Pct Recovery = 79% Analysis Date = 12/14/15 Pct Recovery = 79% Analysis Date = 12/14/15 Pct Recovery = 79% Analysis Date = 12/04/15 Pct Recovery = 79% Analysis Date = 12/04/15 Pct Recovery = 79% Analysis Date = 11/25/15 Pct Recovery = 79% Analysis Date = 11/25/15 Pct Recovery = 79% Analysis Date = 11/15/15 Pct Recovery = 79% Analysis Date = 11/15/15 Pct Recovery = 79% Analysis Date = 11/06/15 Pct Recovery = 79% Analysis Date = 11/06/15 Pct Recovery = 79% Analysis Date = 10/28/15 Pct Recovery = 79% Analysis Date = 10/28/15 Pct Recovery = 79% Analysis Date = 10/18/15 Pct Recovery = 79% Analysis Date = 10/18/15 Pct Recovery = 79% Analysis Date = 10/09/15 Pct Recovery = 79% Analysis Date = 10/09/15 Pct Recovery = 79% Analysis Date = 09/29/15 Pct Recovery = 79% Analysis Date = 09/29/15 Pct Recovery = 79% Analysis Date = 09/20/15 Pct Recovery = 79% Analysis Date = 09/20/15 Pct Recovery = 79% Analysis Date = 09/11/15 Pct Recovery = 78% Analysis Date = 09/11/15 Pct Recovery = 78% Analysis Date = 09/01/15 Pct Recovery = 78% Analysis Date = 09/01/15 Pct Recovery = 78% Analysis Date = 08/23/15 Pct Recovery = 78% Analysis Date = 08/23/15 Pct Recovery = 78% Analysis Date = 08/13/15 Pct Recovery = 78% Analysis Date = 08/13/15 Pct Recovery = 78% Analysis Date = 08/04/15 Pct Recovery = 78% Analysis Date = 08/04/15 Pct Recovery = 78% Analysis Date = 07/26/15 Pct Recovery = 78% Analysis Date = 07/26/15 Pct Recovery = 78% Analysis Date = 07/16/15 Pct Recovery = 78% Analysis Date = 07/16/15 Pct Recovery = 78% Analysis Date = 07/07/15 Pct Recovery = 78% Analysis Date = 07/07/15 Pct Recovery = 78% Analysis Date = 06/28/15 Pct Recovery = 78% Analysis Date = 06/28/15 Pct Recovery = 78% Analysis Date = 06/18/15 Pct Recovery = 78% Analysis Date = 06/18/15 Pct Recovery = 78% Analysis Date = 06/09/15 Pct Recovery = 78% Analysis Date = 06/09/15 Pct Recovery = 78% Analysis Date = 05/30/15 Pct Recovery = 78% Analysis Date = 05/30/15 Pct Recovery = 78% Analysis Date = 05/21/15 Pct Recovery = 78% Analysis Date = 05/21/15 Pct Recovery = 78% Analysis Date = 05/12/15 Pct Recovery = 78% Analysis Date = 05/12/15 Pct Recovery = 78% Analysis Date = 05/02/15 Pct Recovery = 78% Analysis Date = 05/02/15 Pct Recovery = 78% Analysis Date = 04/23/15 Pct Recovery = 78% Analysis Date = 04/23/15 Pct Recovery = 78% Analysis Date = 04/13/15 Pct Recovery = 78% Analysis Date = 04/13/15 Pct Recovery = 78% Analysis Date = 04/04/15 Pct Recovery = 78% Analysis Date = 04/04/15 Pct Recovery = 78% Analysis Date = 03/26/15 Pct Recovery = 78% Analysis Date = 03/26/15 Pct Recovery = 78% Analysis Date = 03/16/15 Pct Recovery = 78% Analysis Date = 03/16/15 Pct Recovery = 78% Analysis Date = 03/07/15 Pct Recovery = 78% Analysis Date = 03/07/15 Pct Recovery = 78% Analysis Date = 02/25/15 Pct Recovery = 78% Analysis Date = 02/25/15 Pct Recovery = 78% Analysis Date = 02/16/15 Pct Recovery = 78% Analysis Date = 02/16/15 Pct Recovery = 78% Analysis Date = 02/07/15 Pct Recovery = 78% Analysis Date = 02/07/15 Pct Recovery = 78% Analysis Date = 01/28/15 Pct Recovery = 78% Analysis Date = 01/28/15 Pct Recovery = 78% Analysis Date = 01/19/15 Pct Recovery = 78% Analysis Date = 01/19/15 Pct Recovery = 78% Analysis Date = 01/10/15 Pct Recovery = 78% Analysis Date = 01/10/15 Pct Recovery = 78% Analysis Date = 12/31/14 Pct Recovery = 78% Analysis Date = 12/31/14 Pct Recovery = 78% Analysis Date = 12/22/14 Pct Recovery = 78% Analysis Date = 12/22/14 Pct Recovery = 78% Analysis Date = 12/12/14 Pct Recovery = 78% Analysis Date = 12/12/14 Pct Recovery = 78% Analysis Date = 12/03/14 Pct Recovery = 78% Analysis Date = 12/03/14 Pct Recovery = 78% Analysis Date = 11/24/14 Pct Recovery = 78% Analysis Date = 11/24/14 Pct Recovery = 78% Analysis Date = 11/14/14 Pct Recovery = 79% Analysis Date = 11/14/14 Pct Recovery = 79% Analysis Date = 11/05/14 Pct Recovery = 79% Analysis Date = 11/05/14 Pct Recovery = 79% Analysis Date = 10/26/14 Pct Recovery = 79% Analysis Date = 10/26/14 Pct Recovery = 79% Analysis Date = 10/17/14 Pct Recovery = 79% Analysis Date = 10/17/14 Pct Recovery = 79% Analysis Date = 10/08/14 Pct Recovery = 79% Analysis Date = 10/08/14 Pct Recovery = 79% Analysis Date = 09/28/14 Pct Recovery = 79% Analysis Date = 09/28/14 Pct Recovery = 79% Analysis Date = 09/19/14 Pct Recovery = 79% Analysis Date = 09/19/14 Pct Recovery = 79% Analysis Date = 09/09/14 Pct Recovery = 79% Analysis Date = 09/09/14 Pct Recovery = 79% Analysis Date = 08/31/14 Pct Recovery = 79% Analysis Date = 08/31/14 Pct Recovery = 79% Analysis Date = 08/22/14 Pct Recovery = 79% Analysis Date = 08/22/14 Pct Recovery = 79% Analysis Date = 08/12/14 Pct Recovery = 79% Analysis Date = 08/12/14 Pct Recovery = 79% Analysis Date = 08/03/14 Pct Recovery = 79% Analysis Date = 08/03/14 Pct Recovery = 79% Analysis Date = 07/25/14 Pct Recovery = 79% Analysis Date = 07/25/14 Pct Recovery = 79% Analysis Date = 07/15/14 Pct Recovery = 79% Analysis Date = 07/15/14 Pct Recovery = 79% Analysis Date = 07/06/14 Pct Recovery = 79% Analysis Date = 07/06/14 Pct Recovery = 79% Analysis Date = 06/26/14 Pct Recovery = 79% Analysis Date = 06/26/14 Pct Recovery = 79% Analysis Date = 06/17/14 Pct Recovery = 79% Analysis Date = 06/17/14 Pct Recovery = 79% Analysis Date = 06/08/14 Pct Recovery = 79% Analysis Date = 06/08/14 Pct Recovery = 79% Analysis Date = 05/29/14 Pct Recovery = 79% Analysis Date = 05/29/14 Pct Recovery = 79% Analysis Date = 05/20/14 Pct Recovery = 79% Analysis Date = 05/20/14 Pct Recovery = 79% Analysis Date = 05/10/14 Pct Recovery = 79% Analysis Date = 05/10/14 Pct Recovery = 79% Analysis Date = 05/01/14 Pct Recovery = 80% Analysis Date = 05/01/14 Pct Recovery = 80% Analysis Date = 04/22/14 Pct Recovery = 80% Analysis Date = 04/22/14 Pct Recovery = 80% Analysis Date = 04/12/14 Pct Recovery = 80% Analysis Date = 04/12/14 Pct Recovery = 80% Analysis Date = 04/03/14 Pct Recovery = 80% Analysis Date = 04/03/14 Pct Recovery = 80% Analysis Date = 03/24/14 Pct Recovery = 80% Analysis Date = 03/24/14 Pct Recovery = 80% Analysis Date = 03/15/14 Pct Recovery = 80% Analysis Date = 03/15/14 Pct Recovery = 80% Analysis Date = 03/06/14 Pct Recovery = 80% Analysis Date = 03/06/14 Pct Recovery = 80% Analysis Date = 02/24/14 Pct Recovery = 80% Analysis Date = 02/24/14 Pct Recovery = 80% Analysis Date = 02/15/14 Pct Recovery = 80% Analysis Date = 02/15/14 Pct Recovery = 80% Analysis Date = 02/05/14 Pct Recovery = 80% Analysis Date = 02/05/14 Pct Recovery = 80% Analysis Date = 01/27/14 Pct Recovery = 80% Analysis Date = 01/27/14 Pct Recovery = 80% Analysis Date = 01/18/14 Pct Recovery = 80% Analysis Date = 01/18/14 Pct Recovery = 80% Analysis Date = 01/08/14 Pct Recovery = 80% Analysis Date = 01/08/14 Pct Recovery = 80% Analysis Date = 12/30/13 Pct Recovery = 80% Analysis Date = 12/30/13 Pct Recovery = 80% Analysis Date = 12/21/13 Pct Recovery = 80% Analysis Date = 12/21/13 Pct Recovery = 80% Analysis Date = 12/11/13 Pct Recovery = 81% Analysis Date = 12/11/13 Pct Recovery = 81% Analysis Date = 12/02/13 Pct Recovery = 81% Analysis Date = 12/02/13 Pct Recovery = 81% Analysis Date = 11/22/13 Pct Recovery = 81% Analysis Date = 11/22/13 Pct Recovery = 81% Analysis Date = 11/13/13 Pct Recovery = 81% Analysis Date = 11/13/13 Pct Recovery = 81% Analysis Date = 11/04/13 Pct Recovery = 81% Analysis Date = 11/04/13 Pct Recovery = 81% Analysis Date = 10/25/13 Pct Recovery = 81% Analysis Date = 10/25/13 Pct Recovery = 81% Analysis Date = 10/16/13 Pct Recovery = 81% Analysis Date = 10/16/13 Pct Recovery = 81% Analysis Date = 10/06/13 Pct Recovery = 81% Analysis Date = 10/06/13 Pct Recovery = 81% Analysis Date = 09/27/13 Pct Recovery = 81% Analysis Date = 09/27/13 Pct Recovery = 81% Analysis Date = 09/18/13 Pct Recovery = 81% Analysis Date = 09/18/13 Pct Recovery = 81% Analysis Date = 09/08/13 Pct Recovery = 81% Analysis Date = 09/08/13 Pct Recovery = 81% Analysis Date = 08/30/13 Pct Recovery = 81% Analysis Date = 08/30/13 Pct Recovery = 81% Analysis Date = 08/20/13 Pct Recovery = 81% Analysis Date = 08/20/13 Pct Recovery = 81% Analysis Date = 08/11/13 Pct Recovery = 81% Analysis Date = 08/11/13 Pct Recovery = 81% Analysis Date = 08/02/13 Pct Recovery = 81% Analysis Date = 08/02/13 Pct Recovery = 81% Analysis Date = 07/23/13 Pct Recovery = 81% Analysis Date = 07/23/13 Pct Recovery = 81% Analysis Date = 07/14/13 Pct Recovery = 82% Analysis Date = 07/14/13 Pct Recovery = 82% Analysis Date = 07/05/13 Pct Recovery = 82% Analysis Date = 07/05/13 Pct Recovery = 82% Analysis Date = 06/25/13 Pct Recovery = 82% Analysis Date = 06/25/13 Pct Recovery = 82% Analysis Date = 06/16/13 Pct Recovery = 82% Analysis Date = 06/16/13 Pct Recovery = 82% Analysis Date = 06/06/13 Pct Recovery = 82% Analysis Date = 06/06/13 Pct Recovery = 82% Analysis Date = 05/28/13 Pct Recovery = 82% Analysis Date = 05/28/13 Pct Recovery = 82% Analysis Date = 05/19/13 Pct Recovery = 82% Analysis Date = 05/19/13 Pct Recovery = 82% Analysis Date = 05/09/13 Pct Recovery = 82% Analysis Date = 05/09/13 Pct Recovery = 82% Analysis Date = 04/30/13 Pct Recovery = 82% Analysis Date = 04/30/13 Pct Recovery = 82% Analysis Date = 04/20/13 Pct Recovery = 82% Analysis Date = 04/20/13 Pct Recovery = 82% Analysis Date = 04/11/13 Pct Recovery = 82% Analysis Date = 04/11/13 Pct Recovery = 82% Analysis Date = 04/02/13 Pct Recovery = 82% Analysis Date = 04/02/13 Pct Recovery = 82% Analysis Date = 03/23/13 Pct Recovery = 82% Analysis Date = 03/23/13 Pct Recovery = 82% Analysis Date = 03/14/13 Pct Recovery = 82% Analysis Date = 03/14/13 Pct Recovery = 82% Analysis Date = 03/04/13 Pct Recovery = 82% Analysis Date = 03/04/13 Pct Recovery = 82% Analysis Date = 02/23/13 Pct Recovery = 82% Analysis Date = 02/23/13 Pct Recovery = 82% Analysis Date = 02/14/13 Pct Recovery = 83% Analysis Date = 02/14/13 Pct Recovery = 83% Analysis Date = 02/04/13 Pct Recovery = 83% Analysis Date = 02/04/13 Pct Recovery = 83% Analysis Date = 01/26/13 Pct Recovery = 83% Analysis Date = 01/26/13 Pct Recovery = 83% Analysis Date = 01/17/13 Pct Recovery = 83% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
TRIFLURALIN

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 78 81% 12% 81% 12%
Total 78 81% 12% 81% 12%

Sample Statistics
TRIFLURALIN

Characteristic N % % Basis
Plotted 78 100% Spiked
Estimated Values 2 3% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 78 .  
False Negatives 0 0% 0 out of 78
Not Spiked 40 .  
False Positives 0 0% 0 out of 40