BQS OBSP Determination:
1,4-DICHLOROBENZENE
METHOD: 5433 , TESTIDCODE: 63163GM008
DATES: 11/09/16 - 03/17/17
Open Data Set

Expected Conc. = 401 Median Pct Recovery = 12% Expected Conc. = 251 Median Pct Recovery = 12% Expected Conc. = 251 Median Pct Recovery = 12% Expected Conc. = 251 Median Pct Recovery = 12% Expected Conc. = 251 Median Pct Recovery = 12% Expected Conc. = 251 Median Pct Recovery = 12% Expected Conc. = 251 Median Pct Recovery = 12% Expected Conc. = 251 Median Pct Recovery = 12% Expected Conc. = 251 Median Pct Recovery = 12% Expected Conc. = 251 Median Pct Recovery = 12% Expected Conc. = 251 Median Pct Recovery = 12% Expected Conc. = 251 Median Pct Recovery = 12% Expected Conc. = 251 Median Pct Recovery = 12% Expected Conc. = 249 Median Pct Recovery = 12% Expected Conc. = 249 Median Pct Recovery = 12% Expected Conc. = 249 Median Pct Recovery = 12% Expected Conc. = 249 Median Pct Recovery = 12% Expected Conc. = 401 Median Pct Recovery = 12% Expected Conc. = 401 Median Pct Recovery = 12% Expected Conc. = 401 Median Pct Recovery = 12% Expected Conc. = 401 Median Pct Recovery = 12% Expected Conc. = 249 Median Pct Recovery = 12% Analysis Date = 03/15/17 SpikeMix = ERA 04121605: 0 µl & Abs 051816sed3H1: 0 µl Pct Recovery = 6% Analysis Date = 03/17/17 SpikeMix = Abs 050916sed3L3: 0 µl & ERA 04121604: 0 µl Pct Recovery = 12% Analysis Date = 03/17/17 SpikeMix = ERA 04121604: 0 µl & ERA 04121605: 0 µl Pct Recovery = 19% Analysis Date = 03/17/17 SpikeMix = ERA 04121606: 0 µl & ERA 04121604: 0 µl Pct Recovery = 16% Analysis Date = 02/21/17 SpikeMix = ERA 04121606: 0 µl & ERA 04121604: 0 µl Pct Recovery = 13% Analysis Date = 02/21/17 SpikeMix = ERA 04121604: 0 µl & Abs 050916sed3L2: 0 µl Pct Recovery = 10% Analysis Date = 02/10/17 SpikeMix = ERA 04121604: 0 µl & ERA 04121605: 0 µl Pct Recovery = 16% Analysis Date = 11/09/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 051816sed3L1: 0 µl Pct Recovery = 9% Analysis Date = 11/09/16 SpikeMix = Abs 051816sed3L1: 0 µl & Abs 050916sed3L2: 0 µl Pct Recovery = 10% Median Pct Recovery = 12% Median Pct Recovery = 12% Median Pct Recovery = 12% Median Pct Recovery = 12% Median Pct Recovery = 12% Median Pct Recovery = 12% Median Pct Recovery = 12% Median Pct Recovery = 12% Median Pct Recovery = 12% Median Pct Recovery = 12% Median Pct Recovery = 12% Median Pct Recovery = 12% Median Pct Recovery = 12% Median Pct Recovery = 12% Median Pct Recovery = 12% Median Pct Recovery = 12% Median Pct Recovery = 12% Median Pct Recovery = 12% Median Pct Recovery = 12% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
1-METHYLNAPHTHALENE
METHOD: 5433 , TESTIDCODE: 63165GM008
DATES: 10/12/16 - 03/17/17
Open Data Set

Expected Conc. = 401 Median Pct Recovery = 34% Expected Conc. = 401 Median Pct Recovery = 34% Expected Conc. = 401 Median Pct Recovery = 34% Expected Conc. = 250 Median Pct Recovery = 34% Expected Conc. = 250 Median Pct Recovery = 34% Expected Conc. = 250 Median Pct Recovery = 34% Expected Conc. = 250 Median Pct Recovery = 34% Expected Conc. = 250 Median Pct Recovery = 34% Expected Conc. = 250 Median Pct Recovery = 34% Expected Conc. = 250 Median Pct Recovery = 34% Expected Conc. = 250 Median Pct Recovery = 34% Expected Conc. = 250 Median Pct Recovery = 34% Expected Conc. = 250 Median Pct Recovery = 34% Expected Conc. = 250 Median Pct Recovery = 34% Expected Conc. = 250 Median Pct Recovery = 34% Expected Conc. = 249 Median Pct Recovery = 34% Expected Conc. = 249 Median Pct Recovery = 34% Expected Conc. = 249 Median Pct Recovery = 34% Expected Conc. = 249 Median Pct Recovery = 34% Expected Conc. = 401 Median Pct Recovery = 34% Expected Conc. = 401 Median Pct Recovery = 34% Expected Conc. = 249 Median Pct Recovery = 34% Analysis Date = 11/09/16 SpikeMix = Abs 050916sed3H2: 0 µl & Abs 050916sed3L3: 0 µl Pct Recovery = 27% Analysis Date = 10/12/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 050916sed3H2: 0 µl Pct Recovery = 36% Analysis Date = 03/17/17 SpikeMix = ERA 04121604: 0 µl & ERA 04121605: 0 µl Pct Recovery = 34% Analysis Date = 03/17/17 SpikeMix = ERA 04121605: 0 µl Pct Recovery = 66% Analysis Date = 03/15/17 SpikeMix = ERA 04121605: 0 µl & ERA 04121606: 0 µl Pct Recovery = 32% Analysis Date = 03/15/17 SpikeMix = ERA 04121605: 0 µl & Abs 051816sed3H1: 0 µl Pct Recovery = 30% Analysis Date = 02/10/17 SpikeMix = ERA 04121604: 0 µl & ERA 04121605: 0 µl Pct Recovery = 35% Analysis Date = 02/10/17 SpikeMix = ERA 04121605: 0 µl & ERA 04121606: 0 µl Pct Recovery = 37% Analysis Date = 02/21/17 SpikeMix = ERA 04121604: 0 µl & Abs 050916sed3L2: 0 µl Pct Recovery = 21% Analysis Date = 11/09/16 SpikeMix = Abs 051816sed3L1: 0 µl & Abs 050916sed3L2: 0 µl Pct Recovery = 35% Median Pct Recovery = 34% Median Pct Recovery = 34% Median Pct Recovery = 34% Median Pct Recovery = 34% Median Pct Recovery = 34% Median Pct Recovery = 34% Median Pct Recovery = 34% Median Pct Recovery = 34% Median Pct Recovery = 34% Median Pct Recovery = 34% Median Pct Recovery = 34% Median Pct Recovery = 34% Median Pct Recovery = 34% Median Pct Recovery = 34% Median Pct Recovery = 34% Median Pct Recovery = 34% Median Pct Recovery = 34% Median Pct Recovery = 34% Median Pct Recovery = 34% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
2,2',4,4'-TETRABROMODIPHENYL ETHER (PBDE 47)
METHOD: 5433 , TESTIDCODE: 63166GM008
DATES: 10/12/16 - 03/17/17
Open Data Set

Expected Conc. = 400 Median Pct Recovery = 41% Expected Conc. = 400 Median Pct Recovery = 41% Expected Conc. = 400 Median Pct Recovery = 41% Expected Conc. = 249 Median Pct Recovery = 41% Expected Conc. = 249 Median Pct Recovery = 41% Expected Conc. = 249 Median Pct Recovery = 41% Expected Conc. = 249 Median Pct Recovery = 41% Expected Conc. = 249 Median Pct Recovery = 41% Expected Conc. = 249 Median Pct Recovery = 41% Expected Conc. = 249 Median Pct Recovery = 41% Expected Conc. = 249 Median Pct Recovery = 41% Expected Conc. = 249 Median Pct Recovery = 41% Expected Conc. = 249 Median Pct Recovery = 41% Expected Conc. = 249 Median Pct Recovery = 41% Expected Conc. = 249 Median Pct Recovery = 41% Expected Conc. = 248 Median Pct Recovery = 41% Expected Conc. = 248 Median Pct Recovery = 41% Expected Conc. = 248 Median Pct Recovery = 41% Expected Conc. = 248 Median Pct Recovery = 41% Expected Conc. = 400 Median Pct Recovery = 41% Expected Conc. = 400 Median Pct Recovery = 41% Expected Conc. = 248 Median Pct Recovery = 41% Analysis Date = 11/09/16 SpikeMix = Abs 050916sed3H2: 0 µl & Abs 050916sed3L3: 0 µl Pct Recovery = 32% Analysis Date = 10/12/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 050916sed3H2: 0 µl Pct Recovery = 40% Analysis Date = 03/17/17 SpikeMix = ERA 04121604: 0 µl & ERA 04121605: 0 µl Pct Recovery = 44% Analysis Date = 03/17/17 SpikeMix = ERA 04121605: 0 µl Pct Recovery = 86% Analysis Date = 03/15/17 SpikeMix = ERA 04121605: 0 µl & ERA 04121606: 0 µl Pct Recovery = 38% Analysis Date = 03/15/17 SpikeMix = ERA 04121605: 0 µl & Abs 051816sed3H1: 0 µl Pct Recovery = 37% Analysis Date = 02/10/17 SpikeMix = ERA 04121604: 0 µl & ERA 04121605: 0 µl Pct Recovery = 45% Analysis Date = 02/10/17 SpikeMix = ERA 04121605: 0 µl & ERA 04121606: 0 µl Pct Recovery = 43% Analysis Date = 02/21/17 SpikeMix = ERA 04121604: 0 µl & Abs 050916sed3L2: 0 µl Pct Recovery = 41% Analysis Date = 11/09/16 SpikeMix = Abs 051816sed3L1: 0 µl & Abs 050916sed3L2: 0 µl Pct Recovery = 36% Median Pct Recovery = 41% Median Pct Recovery = 41% Median Pct Recovery = 41% Median Pct Recovery = 41% Median Pct Recovery = 41% Median Pct Recovery = 41% Median Pct Recovery = 41% Median Pct Recovery = 41% Median Pct Recovery = 41% Median Pct Recovery = 41% Median Pct Recovery = 41% Median Pct Recovery = 41% Median Pct Recovery = 41% Median Pct Recovery = 41% Median Pct Recovery = 41% Median Pct Recovery = 41% Median Pct Recovery = 41% Median Pct Recovery = 41% Median Pct Recovery = 41% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
2,6-DIMETHYLNAPHTHALENE
METHOD: 5433 , TESTIDCODE: 63167GM008
DATES: 10/12/16 - 03/17/17
Open Data Set

Expected Conc. = 401 Median Pct Recovery = 31% Expected Conc. = 401 Median Pct Recovery = 31% Expected Conc. = 401 Median Pct Recovery = 31% Expected Conc. = 401 Median Pct Recovery = 31% Expected Conc. = 401 Median Pct Recovery = 31% Expected Conc. = 252 Median Pct Recovery = 31% Expected Conc. = 252 Median Pct Recovery = 31% Expected Conc. = 252 Median Pct Recovery = 31% Expected Conc. = 252 Median Pct Recovery = 31% Expected Conc. = 252 Median Pct Recovery = 31% Expected Conc. = 252 Median Pct Recovery = 31% Expected Conc. = 252 Median Pct Recovery = 31% Expected Conc. = 252 Median Pct Recovery = 31% Expected Conc. = 252 Median Pct Recovery = 31% Expected Conc. = 252 Median Pct Recovery = 31% Expected Conc. = 249 Median Pct Recovery = 31% Expected Conc. = 249 Median Pct Recovery = 31% Expected Conc. = 249 Median Pct Recovery = 31% Expected Conc. = 249 Median Pct Recovery = 31% Expected Conc. = 252 Median Pct Recovery = 31% Expected Conc. = 252 Median Pct Recovery = 31% Expected Conc. = 249 Median Pct Recovery = 31% Analysis Date = 11/10/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 051816sed3H1: 0 µl Pct Recovery = 13% Analysis Date = 11/09/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 051816sed3L1: 0 µl Pct Recovery = 29% Analysis Date = 10/12/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 050916sed3H2: 0 µl Pct Recovery = 35% Analysis Date = 03/17/17 SpikeMix = ERA 04121606: 0 µl Pct Recovery = 67% Analysis Date = 03/17/17 SpikeMix = ERA 04121606: 0 µl & ERA 04121604: 0 µl Pct Recovery = 29% Analysis Date = 03/15/17 SpikeMix = ERA 04121605: 0 µl & ERA 04121606: 0 µl Pct Recovery = 28% Analysis Date = 02/21/17 SpikeMix = ERA 04121606: 0 µl & ERA 04121604: 0 µl Pct Recovery = 30% Analysis Date = 02/10/17 SpikeMix = ERA 04121605: 0 µl & ERA 04121606: 0 µl Pct Recovery = 36% Analysis Date = 03/17/17 SpikeMix = Abs 050916sed3L3: 0 µl & ERA 04121604: 0 µl Pct Recovery = 32% Analysis Date = 11/09/16 SpikeMix = Abs 050916sed3H2: 0 µl & Abs 050916sed3L3: 0 µl Pct Recovery = 32% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
2-METHYLNAPHTHALENE
METHOD: 5433 , TESTIDCODE: 63168GM008
DATES: 11/09/16 - 03/17/17
Open Data Set

Expected Conc. = 402 Median Pct Recovery = 29% Expected Conc. = 402 Median Pct Recovery = 29% Expected Conc. = 402 Median Pct Recovery = 29% Expected Conc. = 250 Median Pct Recovery = 29% Expected Conc. = 250 Median Pct Recovery = 29% Expected Conc. = 250 Median Pct Recovery = 29% Expected Conc. = 250 Median Pct Recovery = 29% Expected Conc. = 250 Median Pct Recovery = 29% Expected Conc. = 250 Median Pct Recovery = 29% Expected Conc. = 250 Median Pct Recovery = 29% Expected Conc. = 250 Median Pct Recovery = 29% Expected Conc. = 250 Median Pct Recovery = 29% Expected Conc. = 250 Median Pct Recovery = 29% Expected Conc. = 250 Median Pct Recovery = 29% Expected Conc. = 250 Median Pct Recovery = 29% Expected Conc. = 249 Median Pct Recovery = 29% Expected Conc. = 249 Median Pct Recovery = 29% Expected Conc. = 249 Median Pct Recovery = 29% Expected Conc. = 249 Median Pct Recovery = 29% Expected Conc. = 402 Median Pct Recovery = 29% Expected Conc. = 402 Median Pct Recovery = 29% Expected Conc. = 249 Median Pct Recovery = 29% Analysis Date = 03/15/17 SpikeMix = ERA 04121605: 0 µl & Abs 051816sed3H1: 0 µl Pct Recovery = 24% Analysis Date = 11/10/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 051816sed3H1: 0 µl Pct Recovery = 10% Analysis Date = 03/17/17 SpikeMix = Abs 050916sed3L3: 0 µl & ERA 04121604: 0 µl Pct Recovery = 30% Analysis Date = 03/17/17 SpikeMix = ERA 04121604: 0 µl & ERA 04121605: 0 µl Pct Recovery = 30% Analysis Date = 03/17/17 SpikeMix = ERA 04121606: 0 µl & ERA 04121604: 0 µl Pct Recovery = 26% Analysis Date = 02/21/17 SpikeMix = ERA 04121606: 0 µl & ERA 04121604: 0 µl Pct Recovery = 29% Analysis Date = 02/21/17 SpikeMix = ERA 04121604: 0 µl & Abs 050916sed3L2: 0 µl Pct Recovery = 25% Analysis Date = 02/10/17 SpikeMix = ERA 04121604: 0 µl & ERA 04121605: 0 µl Pct Recovery = 31% Analysis Date = 11/09/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 051816sed3L1: 0 µl Pct Recovery = 30% Analysis Date = 11/09/16 SpikeMix = Abs 051816sed3L1: 0 µl & Abs 050916sed3L2: 0 µl Pct Recovery = 33% Median Pct Recovery = 29% Median Pct Recovery = 29% Median Pct Recovery = 29% Median Pct Recovery = 29% Median Pct Recovery = 29% Median Pct Recovery = 29% Median Pct Recovery = 29% Median Pct Recovery = 29% Median Pct Recovery = 29% Median Pct Recovery = 29% Median Pct Recovery = 29% Median Pct Recovery = 29% Median Pct Recovery = 29% Median Pct Recovery = 29% Median Pct Recovery = 29% Median Pct Recovery = 29% Median Pct Recovery = 29% Median Pct Recovery = 29% Median Pct Recovery = 29% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
3-BETA-COPROSTANOL
METHOD: 5433 , TESTIDCODE: 63170GM008
DATES: 10/12/16 - 03/17/17
Open Data Set

Expected Conc. = 4007 Median Pct Recovery = 42% Expected Conc. = 4007 Median Pct Recovery = 42% Expected Conc. = 4007 Median Pct Recovery = 42% Expected Conc. = 4007 Median Pct Recovery = 42% Expected Conc. = 4007 Median Pct Recovery = 42% Expected Conc. = 2509 Median Pct Recovery = 42% Expected Conc. = 2509 Median Pct Recovery = 42% Expected Conc. = 2509 Median Pct Recovery = 42% Expected Conc. = 2509 Median Pct Recovery = 42% Expected Conc. = 2500 Median Pct Recovery = 42% Expected Conc. = 2500 Median Pct Recovery = 42% Expected Conc. = 2500 Median Pct Recovery = 42% Expected Conc. = 2500 Median Pct Recovery = 42% Expected Conc. = 2500 Median Pct Recovery = 42% Expected Conc. = 2500 Median Pct Recovery = 42% Expected Conc. = 2500 Median Pct Recovery = 42% Expected Conc. = 2500 Median Pct Recovery = 42% Expected Conc. = 2500 Median Pct Recovery = 42% Expected Conc. = 2500 Median Pct Recovery = 42% Expected Conc. = 2509 Median Pct Recovery = 42% Expected Conc. = 2509 Median Pct Recovery = 42% Expected Conc. = 2500 Median Pct Recovery = 42% Analysis Date = 11/10/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 051816sed3H1: 0 µl Pct Recovery = 30% Analysis Date = 11/09/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 051816sed3L1: 0 µl Pct Recovery = 37% Analysis Date = 10/12/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 050916sed3H2: 0 µl Pct Recovery = 48% Analysis Date = 03/17/17 SpikeMix = Abs 050916sed3L3: 0 µl & ERA 04121604: 0 µl Pct Recovery = 39% Analysis Date = 11/09/16 SpikeMix = Abs 050916sed3H2: 0 µl & Abs 050916sed3L3: 0 µl Pct Recovery = 39% Analysis Date = 03/17/17 SpikeMix = ERA 04121606: 0 µl Pct Recovery = 52% Analysis Date = 03/17/17 SpikeMix = ERA 04121606: 0 µl & ERA 04121604: 0 µl Pct Recovery = 31% Analysis Date = 03/15/17 SpikeMix = ERA 04121605: 0 µl & ERA 04121606: 0 µl Pct Recovery = 47% Analysis Date = 02/21/17 SpikeMix = ERA 04121606: 0 µl & ERA 04121604: 0 µl Pct Recovery = 44% Analysis Date = 02/10/17 SpikeMix = ERA 04121605: 0 µl & ERA 04121606: 0 µl Pct Recovery = 44% Median Pct Recovery = 42% Median Pct Recovery = 42% Median Pct Recovery = 42% Median Pct Recovery = 42% Median Pct Recovery = 42% Median Pct Recovery = 42% Median Pct Recovery = 42% Median Pct Recovery = 42% Median Pct Recovery = 42% Median Pct Recovery = 42% Median Pct Recovery = 42% Median Pct Recovery = 42% Median Pct Recovery = 42% Median Pct Recovery = 42% Median Pct Recovery = 42% Median Pct Recovery = 42% Median Pct Recovery = 42% Median Pct Recovery = 42% Median Pct Recovery = 42% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
3-METHYL-1(H)-INDOLE (SKATOLE)
METHOD: 5433 , TESTIDCODE: 63171GM008
DATES: 10/12/16 - 03/17/17
Open Data Set

Expected Conc. = 400 Median Pct Recovery = 11% Expected Conc. = 400 Median Pct Recovery = 11% Expected Conc. = 400 Median Pct Recovery = 11% Expected Conc. = 249 Median Pct Recovery = 11% Expected Conc. = 249 Median Pct Recovery = 11% Expected Conc. = 249 Median Pct Recovery = 11% Expected Conc. = 249 Median Pct Recovery = 11% Expected Conc. = 249 Median Pct Recovery = 11% Expected Conc. = 249 Median Pct Recovery = 11% Expected Conc. = 249 Median Pct Recovery = 11% Expected Conc. = 249 Median Pct Recovery = 11% Expected Conc. = 249 Median Pct Recovery = 11% Expected Conc. = 249 Median Pct Recovery = 11% Expected Conc. = 249 Median Pct Recovery = 11% Expected Conc. = 249 Median Pct Recovery = 11% Expected Conc. = 248 Median Pct Recovery = 11% Expected Conc. = 248 Median Pct Recovery = 11% Expected Conc. = 248 Median Pct Recovery = 11% Expected Conc. = 248 Median Pct Recovery = 11% Expected Conc. = 400 Median Pct Recovery = 11% Expected Conc. = 400 Median Pct Recovery = 11% Expected Conc. = 248 Median Pct Recovery = 11% Analysis Date = 11/09/16 SpikeMix = Abs 050916sed3H2: 0 µl & Abs 050916sed3L3: 0 µl Pct Recovery = 4% Analysis Date = 10/12/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 050916sed3H2: 0 µl Pct Recovery = 8% Analysis Date = 03/17/17 SpikeMix = ERA 04121604: 0 µl & ERA 04121605: 0 µl Pct Recovery = 9% Analysis Date = 03/17/17 SpikeMix = ERA 04121605: 0 µl Pct Recovery = 21% Analysis Date = 03/15/17 SpikeMix = ERA 04121605: 0 µl & ERA 04121606: 0 µl Pct Recovery = 23% Analysis Date = 03/15/17 SpikeMix = ERA 04121605: 0 µl & Abs 051816sed3H1: 0 µl Pct Recovery = 12% Analysis Date = 02/10/17 SpikeMix = ERA 04121604: 0 µl & ERA 04121605: 0 µl Pct Recovery = 27% Analysis Date = 02/10/17 SpikeMix = ERA 04121605: 0 µl & ERA 04121606: 0 µl Pct Recovery = 28% Analysis Date = 02/21/17 SpikeMix = ERA 04121604: 0 µl & Abs 050916sed3L2: 0 µl Pct Recovery = 6% Analysis Date = 11/09/16 SpikeMix = Abs 051816sed3L1: 0 µl & Abs 050916sed3L2: 0 µl Pct Recovery = 7% Median Pct Recovery = 11% Median Pct Recovery = 11% Median Pct Recovery = 11% Median Pct Recovery = 11% Median Pct Recovery = 11% Median Pct Recovery = 11% Median Pct Recovery = 11% Median Pct Recovery = 11% Median Pct Recovery = 11% Median Pct Recovery = 11% Median Pct Recovery = 11% Median Pct Recovery = 11% Median Pct Recovery = 11% Median Pct Recovery = 11% Median Pct Recovery = 11% Median Pct Recovery = 11% Median Pct Recovery = 11% Median Pct Recovery = 11% Median Pct Recovery = 11% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
3-TERT-BUTLY-4-HYDROXY ANISOLE (BHA)
METHOD: 5433 , TESTIDCODE: 63172GM008
DATES: 10/12/16 - 02/21/17
Open Data Set

Expected Conc. = 1207 Median Pct Recovery = 4% Expected Conc. = 1207 Median Pct Recovery = 4% Expected Conc. = 1207 Median Pct Recovery = 4% Expected Conc. = 1207 Median Pct Recovery = 4% Expected Conc. = 1207 Median Pct Recovery = 4% Expected Conc. = 761 Median Pct Recovery = 4% Expected Conc. = 761 Median Pct Recovery = 4% Expected Conc. = 749 Median Pct Recovery = 4% Expected Conc. = 749 Median Pct Recovery = 4% Expected Conc. = 761 Median Pct Recovery = 4% Expected Conc. = 761 Median Pct Recovery = 4% Expected Conc. = 761 Median Pct Recovery = 4% Expected Conc. = 761 Median Pct Recovery = 4% Expected Conc. = 749 Median Pct Recovery = 4% Expected Conc. = 749 Median Pct Recovery = 4% Expected Conc. = 749 Median Pct Recovery = 4% Expected Conc. = 749 Median Pct Recovery = 4% Expected Conc. = 749 Median Pct Recovery = 4% Expected Conc. = 749 Median Pct Recovery = 4% Expected Conc. = 749 Median Pct Recovery = 4% Expected Conc. = 749 Median Pct Recovery = 4% Expected Conc. = 749 Median Pct Recovery = 4% Analysis Date = 11/10/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 051816sed3H1: 0 µl Pct Recovery = 3% Analysis Date = 11/09/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 051816sed3L1: 0 µl Pct Recovery = 6% Analysis Date = 10/12/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 050916sed3H2: 0 µl Pct Recovery = 12% Analysis Date = 11/09/16 SpikeMix = Abs 050916sed3H2: 0 µl & Abs 050916sed3L3: 0 µl Pct Recovery = 4% Analysis Date = 02/21/17 SpikeMix = ERA 04121606: 0 µl & ERA 04121604: 0 µl Pct Recovery = 2% Median Pct Recovery = 4% Median Pct Recovery = 4% Median Pct Recovery = 4% Median Pct Recovery = 4% Median Pct Recovery = 4% Median Pct Recovery = 4% Median Pct Recovery = 4% Median Pct Recovery = 4% Median Pct Recovery = 4% Median Pct Recovery = 4% Median Pct Recovery = 4% Median Pct Recovery = 4% Median Pct Recovery = 4% Median Pct Recovery = 4% Median Pct Recovery = 4% Median Pct Recovery = 4% Median Pct Recovery = 4% Median Pct Recovery = 4% Median Pct Recovery = 4% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
4-CUMYLPHENOL
METHOD: 5433 , TESTIDCODE: 63173GM008
DATES: 10/12/16 - 03/17/17
Open Data Set

Expected Conc. = 403 Median Pct Recovery = 43% Expected Conc. = 403 Median Pct Recovery = 43% Expected Conc. = 403 Median Pct Recovery = 43% Expected Conc. = 250 Median Pct Recovery = 43% Expected Conc. = 250 Median Pct Recovery = 43% Expected Conc. = 250 Median Pct Recovery = 43% Expected Conc. = 250 Median Pct Recovery = 43% Expected Conc. = 249 Median Pct Recovery = 43% Expected Conc. = 249 Median Pct Recovery = 43% Expected Conc. = 249 Median Pct Recovery = 43% Expected Conc. = 249 Median Pct Recovery = 43% Expected Conc. = 249 Median Pct Recovery = 43% Expected Conc. = 249 Median Pct Recovery = 43% Expected Conc. = 249 Median Pct Recovery = 43% Expected Conc. = 249 Median Pct Recovery = 43% Expected Conc. = 249 Median Pct Recovery = 43% Expected Conc. = 249 Median Pct Recovery = 43% Expected Conc. = 249 Median Pct Recovery = 43% Expected Conc. = 249 Median Pct Recovery = 43% Expected Conc. = 403 Median Pct Recovery = 43% Expected Conc. = 403 Median Pct Recovery = 43% Expected Conc. = 250 Median Pct Recovery = 43% Analysis Date = 11/09/16 SpikeMix = Abs 050916sed3H2: 0 µl & Abs 050916sed3L3: 0 µl Pct Recovery = 41% Analysis Date = 10/12/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 050916sed3H2: 0 µl Pct Recovery = 48% Analysis Date = 02/21/17 SpikeMix = ERA 04121604: 0 µl & Abs 050916sed3L2: 0 µl Pct Recovery = 45% Analysis Date = 11/09/16 SpikeMix = Abs 051816sed3L1: 0 µl & Abs 050916sed3L2: 0 µl Pct Recovery = 45% Analysis Date = 03/17/17 SpikeMix = ERA 04121604: 0 µl & ERA 04121605: 0 µl Pct Recovery = 29% Analysis Date = 03/17/17 SpikeMix = ERA 04121605: 0 µl Pct Recovery = 63% Analysis Date = 03/15/17 SpikeMix = ERA 04121605: 0 µl & ERA 04121606: 0 µl Pct Recovery = 39% Analysis Date = 03/15/17 SpikeMix = ERA 04121605: 0 µl & Abs 051816sed3H1: 0 µl Pct Recovery = 40% Analysis Date = 02/10/17 SpikeMix = ERA 04121604: 0 µl & ERA 04121605: 0 µl Pct Recovery = 42% Analysis Date = 02/10/17 SpikeMix = ERA 04121605: 0 µl & ERA 04121606: 0 µl Pct Recovery = 43% Median Pct Recovery = 43% Median Pct Recovery = 43% Median Pct Recovery = 43% Median Pct Recovery = 43% Median Pct Recovery = 43% Median Pct Recovery = 43% Median Pct Recovery = 43% Median Pct Recovery = 43% Median Pct Recovery = 43% Median Pct Recovery = 43% Median Pct Recovery = 43% Median Pct Recovery = 43% Median Pct Recovery = 43% Median Pct Recovery = 43% Median Pct Recovery = 43% Median Pct Recovery = 43% Median Pct Recovery = 43% Median Pct Recovery = 43% Median Pct Recovery = 43% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
4-N-OCTYLPHENOL
METHOD: 5433 , TESTIDCODE: 63174GM008
DATES: 10/12/16 - 03/17/17
Open Data Set

Expected Conc. = 401 Median Pct Recovery = 36% Expected Conc. = 401 Median Pct Recovery = 36% Expected Conc. = 401 Median Pct Recovery = 36% Expected Conc. = 401 Median Pct Recovery = 36% Expected Conc. = 401 Median Pct Recovery = 36% Expected Conc. = 249 Median Pct Recovery = 36% Expected Conc. = 249 Median Pct Recovery = 36% Expected Conc. = 249 Median Pct Recovery = 36% Expected Conc. = 249 Median Pct Recovery = 36% Expected Conc. = 249 Median Pct Recovery = 36% Expected Conc. = 249 Median Pct Recovery = 36% Expected Conc. = 249 Median Pct Recovery = 36% Expected Conc. = 249 Median Pct Recovery = 36% Expected Conc. = 249 Median Pct Recovery = 36% Expected Conc. = 249 Median Pct Recovery = 36% Expected Conc. = 248 Median Pct Recovery = 36% Expected Conc. = 248 Median Pct Recovery = 36% Expected Conc. = 248 Median Pct Recovery = 36% Expected Conc. = 248 Median Pct Recovery = 36% Expected Conc. = 249 Median Pct Recovery = 36% Expected Conc. = 249 Median Pct Recovery = 36% Expected Conc. = 248 Median Pct Recovery = 36% Analysis Date = 11/10/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 051816sed3H1: 0 µl Pct Recovery = 24% Analysis Date = 11/09/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 051816sed3L1: 0 µl Pct Recovery = 39% Analysis Date = 10/12/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 050916sed3H2: 0 µl Pct Recovery = 41% Analysis Date = 03/17/17 SpikeMix = ERA 04121606: 0 µl Pct Recovery = 49% Analysis Date = 03/17/17 SpikeMix = ERA 04121606: 0 µl & ERA 04121604: 0 µl Pct Recovery = 26% Analysis Date = 03/15/17 SpikeMix = ERA 04121605: 0 µl & ERA 04121606: 0 µl Pct Recovery = 28% Analysis Date = 02/21/17 SpikeMix = ERA 04121606: 0 µl & ERA 04121604: 0 µl Pct Recovery = 30% Analysis Date = 02/10/17 SpikeMix = ERA 04121605: 0 µl & ERA 04121606: 0 µl Pct Recovery = 34% Analysis Date = 03/17/17 SpikeMix = Abs 050916sed3L3: 0 µl & ERA 04121604: 0 µl Pct Recovery = 38% Analysis Date = 11/09/16 SpikeMix = Abs 050916sed3H2: 0 µl & Abs 050916sed3L3: 0 µl Pct Recovery = 40% Median Pct Recovery = 36% Median Pct Recovery = 36% Median Pct Recovery = 36% Median Pct Recovery = 36% Median Pct Recovery = 36% Median Pct Recovery = 36% Median Pct Recovery = 36% Median Pct Recovery = 36% Median Pct Recovery = 36% Median Pct Recovery = 36% Median Pct Recovery = 36% Median Pct Recovery = 36% Median Pct Recovery = 36% Median Pct Recovery = 36% Median Pct Recovery = 36% Median Pct Recovery = 36% Median Pct Recovery = 36% Median Pct Recovery = 36% Median Pct Recovery = 36% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
4-TERT-OCTYLPHENOL
METHOD: 5433 , TESTIDCODE: 63176GM008
DATES: 11/09/16 - 03/17/17
Open Data Set

Expected Conc. = 401 Median Pct Recovery = 44% Expected Conc. = 401 Median Pct Recovery = 44% Expected Conc. = 401 Median Pct Recovery = 44% Expected Conc. = 250 Median Pct Recovery = 44% Expected Conc. = 250 Median Pct Recovery = 44% Expected Conc. = 250 Median Pct Recovery = 44% Expected Conc. = 250 Median Pct Recovery = 44% Expected Conc. = 250 Median Pct Recovery = 44% Expected Conc. = 250 Median Pct Recovery = 44% Expected Conc. = 250 Median Pct Recovery = 44% Expected Conc. = 250 Median Pct Recovery = 44% Expected Conc. = 250 Median Pct Recovery = 44% Expected Conc. = 250 Median Pct Recovery = 44% Expected Conc. = 250 Median Pct Recovery = 44% Expected Conc. = 250 Median Pct Recovery = 44% Expected Conc. = 248 Median Pct Recovery = 44% Expected Conc. = 248 Median Pct Recovery = 44% Expected Conc. = 248 Median Pct Recovery = 44% Expected Conc. = 248 Median Pct Recovery = 44% Expected Conc. = 401 Median Pct Recovery = 44% Expected Conc. = 401 Median Pct Recovery = 44% Expected Conc. = 248 Median Pct Recovery = 44% Analysis Date = 03/15/17 SpikeMix = ERA 04121605: 0 µl & Abs 051816sed3H1: 0 µl Pct Recovery = 46% Analysis Date = 11/10/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 051816sed3H1: 0 µl Pct Recovery = 30% Analysis Date = 03/17/17 SpikeMix = Abs 050916sed3L3: 0 µl & ERA 04121604: 0 µl Pct Recovery = 43% Analysis Date = 03/17/17 SpikeMix = ERA 04121604: 0 µl & ERA 04121605: 0 µl Pct Recovery = 23% Analysis Date = 03/17/17 SpikeMix = ERA 04121606: 0 µl & ERA 04121604: 0 µl Pct Recovery = 38% Analysis Date = 02/21/17 SpikeMix = ERA 04121606: 0 µl & ERA 04121604: 0 µl Pct Recovery = 44% Analysis Date = 02/21/17 SpikeMix = ERA 04121604: 0 µl & Abs 050916sed3L2: 0 µl Pct Recovery = 49% Analysis Date = 02/10/17 SpikeMix = ERA 04121604: 0 µl & ERA 04121605: 0 µl Pct Recovery = 44% Analysis Date = 11/09/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 051816sed3L1: 0 µl Pct Recovery = 48% Analysis Date = 11/09/16 SpikeMix = Abs 051816sed3L1: 0 µl & Abs 050916sed3L2: 0 µl Pct Recovery = 49% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
ACETOPHENONE
METHOD: 5433 , TESTIDCODE: 63178GM008
DATES: 10/12/16 - 03/17/17
Open Data Set

Expected Conc. = 1220 Median Pct Recovery = 27% Expected Conc. = 1220 Median Pct Recovery = 27% Expected Conc. = 1220 Median Pct Recovery = 27% Expected Conc. = 1220 Median Pct Recovery = 27% Expected Conc. = 1220 Median Pct Recovery = 27% Expected Conc. = 760 Median Pct Recovery = 27% Expected Conc. = 760 Median Pct Recovery = 27% Expected Conc. = 760 Median Pct Recovery = 27% Expected Conc. = 760 Median Pct Recovery = 27% Expected Conc. = 756 Median Pct Recovery = 27% Expected Conc. = 756 Median Pct Recovery = 27% Expected Conc. = 756 Median Pct Recovery = 27% Expected Conc. = 756 Median Pct Recovery = 27% Expected Conc. = 756 Median Pct Recovery = 27% Expected Conc. = 756 Median Pct Recovery = 27% Expected Conc. = 756 Median Pct Recovery = 27% Expected Conc. = 756 Median Pct Recovery = 27% Expected Conc. = 756 Median Pct Recovery = 27% Expected Conc. = 756 Median Pct Recovery = 27% Expected Conc. = 760 Median Pct Recovery = 27% Expected Conc. = 760 Median Pct Recovery = 27% Expected Conc. = 756 Median Pct Recovery = 27% Analysis Date = 11/10/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 051816sed3H1: 0 µl Pct Recovery = 10% Analysis Date = 11/09/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 051816sed3L1: 0 µl Pct Recovery = 15% Analysis Date = 10/12/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 050916sed3H2: 0 µl Pct Recovery = 17% Analysis Date = 03/17/17 SpikeMix = Abs 050916sed3L3: 0 µl & ERA 04121604: 0 µl Pct Recovery = 17% Analysis Date = 11/09/16 SpikeMix = Abs 050916sed3H2: 0 µl & Abs 050916sed3L3: 0 µl Pct Recovery = 16% Analysis Date = 03/17/17 SpikeMix = ERA 04121606: 0 µl Pct Recovery = 87% Analysis Date = 03/17/17 SpikeMix = ERA 04121606: 0 µl & ERA 04121604: 0 µl Pct Recovery = 38% Analysis Date = 03/15/17 SpikeMix = ERA 04121605: 0 µl & ERA 04121606: 0 µl Pct Recovery = 46% Analysis Date = 02/21/17 SpikeMix = ERA 04121606: 0 µl & ERA 04121604: 0 µl Pct Recovery = 44% Analysis Date = 02/10/17 SpikeMix = ERA 04121605: 0 µl & ERA 04121606: 0 µl Pct Recovery = 44% Median Pct Recovery = 27% Median Pct Recovery = 27% Median Pct Recovery = 27% Median Pct Recovery = 27% Median Pct Recovery = 27% Median Pct Recovery = 27% Median Pct Recovery = 27% Median Pct Recovery = 27% Median Pct Recovery = 27% Median Pct Recovery = 27% Median Pct Recovery = 27% Median Pct Recovery = 27% Median Pct Recovery = 27% Median Pct Recovery = 27% Median Pct Recovery = 27% Median Pct Recovery = 27% Median Pct Recovery = 27% Median Pct Recovery = 27% Median Pct Recovery = 27% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
ACETYL HEXAMETHYL TETRAHYDRONAPHTHALENE (AHTN)
METHOD: 5433 , TESTIDCODE: 63179GM008
DATES: 10/12/16 - 03/17/17
Open Data Set

Expected Conc. = 400 Median Pct Recovery = 40% Expected Conc. = 400 Median Pct Recovery = 40% Expected Conc. = 400 Median Pct Recovery = 40% Expected Conc. = 400 Median Pct Recovery = 40% Expected Conc. = 400 Median Pct Recovery = 40% Expected Conc. = 249 Median Pct Recovery = 40% Expected Conc. = 249 Median Pct Recovery = 40% Expected Conc. = 249 Median Pct Recovery = 40% Expected Conc. = 249 Median Pct Recovery = 40% Expected Conc. = 249 Median Pct Recovery = 40% Expected Conc. = 249 Median Pct Recovery = 40% Expected Conc. = 249 Median Pct Recovery = 40% Expected Conc. = 249 Median Pct Recovery = 40% Expected Conc. = 249 Median Pct Recovery = 40% Expected Conc. = 249 Median Pct Recovery = 40% Expected Conc. = 248 Median Pct Recovery = 40% Expected Conc. = 248 Median Pct Recovery = 40% Expected Conc. = 248 Median Pct Recovery = 40% Expected Conc. = 248 Median Pct Recovery = 40% Expected Conc. = 249 Median Pct Recovery = 40% Expected Conc. = 249 Median Pct Recovery = 40% Expected Conc. = 248 Median Pct Recovery = 40% Analysis Date = 11/10/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 051816sed3H1: 0 µl Pct Recovery = 23% Analysis Date = 11/09/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 051816sed3L1: 0 µl Pct Recovery = 39% Analysis Date = 10/12/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 050916sed3H2: 0 µl Pct Recovery = 44% Analysis Date = 03/17/17 SpikeMix = ERA 04121606: 0 µl Pct Recovery = 78% Analysis Date = 03/17/17 SpikeMix = ERA 04121606: 0 µl & ERA 04121604: 0 µl Pct Recovery = 39% Analysis Date = 03/15/17 SpikeMix = ERA 04121605: 0 µl & ERA 04121606: 0 µl Pct Recovery = 38% Analysis Date = 02/21/17 SpikeMix = ERA 04121606: 0 µl & ERA 04121604: 0 µl Pct Recovery = 40% Analysis Date = 02/10/17 SpikeMix = ERA 04121605: 0 µl & ERA 04121606: 0 µl Pct Recovery = 41% Analysis Date = 03/17/17 SpikeMix = Abs 050916sed3L3: 0 µl & ERA 04121604: 0 µl Pct Recovery = 42% Analysis Date = 11/09/16 SpikeMix = Abs 050916sed3H2: 0 µl & Abs 050916sed3L3: 0 µl Pct Recovery = 43% Median Pct Recovery = 40% Median Pct Recovery = 40% Median Pct Recovery = 40% Median Pct Recovery = 40% Median Pct Recovery = 40% Median Pct Recovery = 40% Median Pct Recovery = 40% Median Pct Recovery = 40% Median Pct Recovery = 40% Median Pct Recovery = 40% Median Pct Recovery = 40% Median Pct Recovery = 40% Median Pct Recovery = 40% Median Pct Recovery = 40% Median Pct Recovery = 40% Median Pct Recovery = 40% Median Pct Recovery = 40% Median Pct Recovery = 40% Median Pct Recovery = 40% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
ANTHRACENE
METHOD: 5433 , TESTIDCODE: 63180GM008
DATES: 10/12/16 - 03/17/17
Open Data Set

Expected Conc. = 401 Median Pct Recovery = 34% Expected Conc. = 401 Median Pct Recovery = 34% Expected Conc. = 401 Median Pct Recovery = 34% Expected Conc. = 252 Median Pct Recovery = 34% Expected Conc. = 252 Median Pct Recovery = 34% Expected Conc. = 252 Median Pct Recovery = 34% Expected Conc. = 252 Median Pct Recovery = 34% Expected Conc. = 252 Median Pct Recovery = 34% Expected Conc. = 252 Median Pct Recovery = 34% Expected Conc. = 252 Median Pct Recovery = 34% Expected Conc. = 252 Median Pct Recovery = 34% Expected Conc. = 252 Median Pct Recovery = 34% Expected Conc. = 252 Median Pct Recovery = 34% Expected Conc. = 252 Median Pct Recovery = 34% Expected Conc. = 252 Median Pct Recovery = 34% Expected Conc. = 248 Median Pct Recovery = 34% Expected Conc. = 248 Median Pct Recovery = 34% Expected Conc. = 248 Median Pct Recovery = 34% Expected Conc. = 248 Median Pct Recovery = 34% Expected Conc. = 401 Median Pct Recovery = 34% Expected Conc. = 401 Median Pct Recovery = 34% Expected Conc. = 248 Median Pct Recovery = 34% Analysis Date = 11/09/16 SpikeMix = Abs 050916sed3H2: 0 µl & Abs 050916sed3L3: 0 µl Pct Recovery = 27% Analysis Date = 10/12/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 050916sed3H2: 0 µl Pct Recovery = 32% Analysis Date = 03/17/17 SpikeMix = ERA 04121604: 0 µl & ERA 04121605: 0 µl Pct Recovery = 33% Analysis Date = 03/17/17 SpikeMix = ERA 04121605: 0 µl Pct Recovery = 65% Analysis Date = 03/15/17 SpikeMix = ERA 04121605: 0 µl & ERA 04121606: 0 µl Pct Recovery = 35% Analysis Date = 03/15/17 SpikeMix = ERA 04121605: 0 µl & Abs 051816sed3H1: 0 µl Pct Recovery = 36% Analysis Date = 02/10/17 SpikeMix = ERA 04121604: 0 µl & ERA 04121605: 0 µl Pct Recovery = 41% Analysis Date = 02/10/17 SpikeMix = ERA 04121605: 0 µl & ERA 04121606: 0 µl Pct Recovery = 42% Analysis Date = 02/21/17 SpikeMix = ERA 04121604: 0 µl & Abs 050916sed3L2: 0 µl Pct Recovery = 28% Analysis Date = 11/09/16 SpikeMix = Abs 051816sed3L1: 0 µl & Abs 050916sed3L2: 0 µl Pct Recovery = 31% Median Pct Recovery = 34% Median Pct Recovery = 34% Median Pct Recovery = 34% Median Pct Recovery = 34% Median Pct Recovery = 34% Median Pct Recovery = 34% Median Pct Recovery = 34% Median Pct Recovery = 34% Median Pct Recovery = 34% Median Pct Recovery = 34% Median Pct Recovery = 34% Median Pct Recovery = 34% Median Pct Recovery = 34% Median Pct Recovery = 34% Median Pct Recovery = 34% Median Pct Recovery = 34% Median Pct Recovery = 34% Median Pct Recovery = 34% Median Pct Recovery = 34% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
ANTHRAQUINONE
METHOD: 5433 , TESTIDCODE: 63181GM008
DATES: 10/12/16 - 03/17/17
Open Data Set

Expected Conc. = 401 Median Pct Recovery = 28% Expected Conc. = 401 Median Pct Recovery = 28% Expected Conc. = 401 Median Pct Recovery = 28% Expected Conc. = 401 Median Pct Recovery = 28% Expected Conc. = 401 Median Pct Recovery = 28% Expected Conc. = 250 Median Pct Recovery = 28% Expected Conc. = 250 Median Pct Recovery = 28% Expected Conc. = 250 Median Pct Recovery = 28% Expected Conc. = 250 Median Pct Recovery = 28% Expected Conc. = 250 Median Pct Recovery = 28% Expected Conc. = 250 Median Pct Recovery = 28% Expected Conc. = 250 Median Pct Recovery = 28% Expected Conc. = 250 Median Pct Recovery = 28% Expected Conc. = 250 Median Pct Recovery = 28% Expected Conc. = 250 Median Pct Recovery = 28% Expected Conc. = 249 Median Pct Recovery = 28% Expected Conc. = 249 Median Pct Recovery = 28% Expected Conc. = 249 Median Pct Recovery = 28% Expected Conc. = 249 Median Pct Recovery = 28% Expected Conc. = 250 Median Pct Recovery = 28% Expected Conc. = 250 Median Pct Recovery = 28% Expected Conc. = 249 Median Pct Recovery = 28% Analysis Date = 11/10/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 051816sed3H1: 0 µl Pct Recovery = 110% Analysis Date = 11/09/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 051816sed3L1: 0 µl Pct Recovery = 32% Analysis Date = 10/12/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 050916sed3H2: 0 µl Pct Recovery = 30% Analysis Date = 03/17/17 SpikeMix = ERA 04121606: 0 µl Pct Recovery = 26% Analysis Date = 03/17/17 SpikeMix = ERA 04121606: 0 µl & ERA 04121604: 0 µl Pct Recovery = 14% Analysis Date = 03/15/17 SpikeMix = ERA 04121605: 0 µl & ERA 04121606: 0 µl Pct Recovery = 16% Analysis Date = 02/21/17 SpikeMix = ERA 04121606: 0 µl & ERA 04121604: 0 µl Pct Recovery = 15% Analysis Date = 02/10/17 SpikeMix = ERA 04121605: 0 µl & ERA 04121606: 0 µl Pct Recovery = 24% Analysis Date = 03/17/17 SpikeMix = Abs 050916sed3L3: 0 µl & ERA 04121604: 0 µl Pct Recovery = 31% Analysis Date = 11/09/16 SpikeMix = Abs 050916sed3H2: 0 µl & Abs 050916sed3L3: 0 µl Pct Recovery = 37% Median Pct Recovery = 28% Median Pct Recovery = 28% Median Pct Recovery = 28% Median Pct Recovery = 28% Median Pct Recovery = 28% Median Pct Recovery = 28% Median Pct Recovery = 28% Median Pct Recovery = 28% Median Pct Recovery = 28% Median Pct Recovery = 28% Median Pct Recovery = 28% Median Pct Recovery = 28% Median Pct Recovery = 28% Median Pct Recovery = 28% Median Pct Recovery = 28% Median Pct Recovery = 28% Median Pct Recovery = 28% Median Pct Recovery = 28% Median Pct Recovery = 28% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
ATRAZINE
METHOD: 5433 , TESTIDCODE: 63182GM008
DATES: 11/09/16 - 03/17/17
Open Data Set

Expected Conc. = 802 Median Pct Recovery = 35% Expected Conc. = 802 Median Pct Recovery = 35% Expected Conc. = 802 Median Pct Recovery = 35% Expected Conc. = 505 Median Pct Recovery = 35% Expected Conc. = 505 Median Pct Recovery = 35% Expected Conc. = 505 Median Pct Recovery = 35% Expected Conc. = 505 Median Pct Recovery = 35% Expected Conc. = 499 Median Pct Recovery = 35% Expected Conc. = 499 Median Pct Recovery = 35% Expected Conc. = 499 Median Pct Recovery = 35% Expected Conc. = 499 Median Pct Recovery = 35% Expected Conc. = 499 Median Pct Recovery = 35% Expected Conc. = 499 Median Pct Recovery = 35% Expected Conc. = 499 Median Pct Recovery = 35% Expected Conc. = 499 Median Pct Recovery = 35% Expected Conc. = 499 Median Pct Recovery = 35% Expected Conc. = 499 Median Pct Recovery = 35% Expected Conc. = 499 Median Pct Recovery = 35% Expected Conc. = 499 Median Pct Recovery = 35% Expected Conc. = 802 Median Pct Recovery = 35% Expected Conc. = 802 Median Pct Recovery = 35% Expected Conc. = 505 Median Pct Recovery = 35% Analysis Date = 03/15/17 SpikeMix = ERA 04121605: 0 µl & Abs 051816sed3H1: 0 µl Pct Recovery = 29% Analysis Date = 11/10/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 051816sed3H1: 0 µl Pct Recovery = 11% Analysis Date = 11/09/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 051816sed3L1: 0 µl Pct Recovery = 31% Analysis Date = 11/09/16 SpikeMix = Abs 051816sed3L1: 0 µl & Abs 050916sed3L2: 0 µl Pct Recovery = 32% Analysis Date = 03/17/17 SpikeMix = Abs 050916sed3L3: 0 µl & ERA 04121604: 0 µl Pct Recovery = 32% Analysis Date = 03/17/17 SpikeMix = ERA 04121604: 0 µl & ERA 04121605: 0 µl Pct Recovery = 39% Analysis Date = 03/17/17 SpikeMix = ERA 04121606: 0 µl & ERA 04121604: 0 µl Pct Recovery = 37% Analysis Date = 02/21/17 SpikeMix = ERA 04121606: 0 µl & ERA 04121604: 0 µl Pct Recovery = 46% Analysis Date = 02/21/17 SpikeMix = ERA 04121604: 0 µl & Abs 050916sed3L2: 0 µl Pct Recovery = 42% Analysis Date = 02/10/17 SpikeMix = ERA 04121604: 0 µl & ERA 04121605: 0 µl Pct Recovery = 43% Median Pct Recovery = 35% Median Pct Recovery = 35% Median Pct Recovery = 35% Median Pct Recovery = 35% Median Pct Recovery = 35% Median Pct Recovery = 35% Median Pct Recovery = 35% Median Pct Recovery = 35% Median Pct Recovery = 35% Median Pct Recovery = 35% Median Pct Recovery = 35% Median Pct Recovery = 35% Median Pct Recovery = 35% Median Pct Recovery = 35% Median Pct Recovery = 35% Median Pct Recovery = 35% Median Pct Recovery = 35% Median Pct Recovery = 35% Median Pct Recovery = 35% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
BENZO[A]PYRENE
METHOD: 5433 , TESTIDCODE: 63183GM008
DATES: 10/12/16 - 03/17/17
Open Data Set

Expected Conc. = 403 Median Pct Recovery = 39% Expected Conc. = 403 Median Pct Recovery = 39% Expected Conc. = 403 Median Pct Recovery = 39% Expected Conc. = 403 Median Pct Recovery = 39% Expected Conc. = 403 Median Pct Recovery = 39% Expected Conc. = 251 Median Pct Recovery = 39% Expected Conc. = 251 Median Pct Recovery = 39% Expected Conc. = 251 Median Pct Recovery = 39% Expected Conc. = 251 Median Pct Recovery = 39% Expected Conc. = 251 Median Pct Recovery = 39% Expected Conc. = 251 Median Pct Recovery = 39% Expected Conc. = 251 Median Pct Recovery = 39% Expected Conc. = 251 Median Pct Recovery = 39% Expected Conc. = 251 Median Pct Recovery = 39% Expected Conc. = 251 Median Pct Recovery = 39% Expected Conc. = 250 Median Pct Recovery = 39% Expected Conc. = 250 Median Pct Recovery = 39% Expected Conc. = 250 Median Pct Recovery = 39% Expected Conc. = 250 Median Pct Recovery = 39% Expected Conc. = 251 Median Pct Recovery = 39% Expected Conc. = 251 Median Pct Recovery = 39% Expected Conc. = 250 Median Pct Recovery = 39% Analysis Date = 11/10/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 051816sed3H1: 0 µl Pct Recovery = 99% Analysis Date = 11/09/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 051816sed3L1: 0 µl Pct Recovery = 38% Analysis Date = 10/12/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 050916sed3H2: 0 µl Pct Recovery = 43% Analysis Date = 03/17/17 SpikeMix = ERA 04121606: 0 µl Pct Recovery = 73% Analysis Date = 03/17/17 SpikeMix = ERA 04121606: 0 µl & ERA 04121604: 0 µl Pct Recovery = 33% Analysis Date = 03/15/17 SpikeMix = ERA 04121605: 0 µl & ERA 04121606: 0 µl Pct Recovery = 35% Analysis Date = 02/21/17 SpikeMix = ERA 04121606: 0 µl & ERA 04121604: 0 µl Pct Recovery = 37% Analysis Date = 02/10/17 SpikeMix = ERA 04121605: 0 µl & ERA 04121606: 0 µl Pct Recovery = 45% Analysis Date = 03/17/17 SpikeMix = Abs 050916sed3L3: 0 µl & ERA 04121604: 0 µl Pct Recovery = 38% Analysis Date = 11/09/16 SpikeMix = Abs 050916sed3H2: 0 µl & Abs 050916sed3L3: 0 µl Pct Recovery = 39% Median Pct Recovery = 39% Median Pct Recovery = 39% Median Pct Recovery = 39% Median Pct Recovery = 39% Median Pct Recovery = 39% Median Pct Recovery = 39% Median Pct Recovery = 39% Median Pct Recovery = 39% Median Pct Recovery = 39% Median Pct Recovery = 39% Median Pct Recovery = 39% Median Pct Recovery = 39% Median Pct Recovery = 39% Median Pct Recovery = 39% Median Pct Recovery = 39% Median Pct Recovery = 39% Median Pct Recovery = 39% Median Pct Recovery = 39% Median Pct Recovery = 39% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
BENZOPHENONE
METHOD: 5433 , TESTIDCODE: 63184GM008
DATES: 10/12/16 - 03/17/17
Open Data Set

Expected Conc. = 402 Median Pct Recovery = 50% Expected Conc. = 402 Median Pct Recovery = 50% Expected Conc. = 402 Median Pct Recovery = 50% Expected Conc. = 252 Median Pct Recovery = 50% Expected Conc. = 252 Median Pct Recovery = 50% Expected Conc. = 252 Median Pct Recovery = 50% Expected Conc. = 252 Median Pct Recovery = 50% Expected Conc. = 252 Median Pct Recovery = 50% Expected Conc. = 252 Median Pct Recovery = 50% Expected Conc. = 252 Median Pct Recovery = 50% Expected Conc. = 252 Median Pct Recovery = 50% Expected Conc. = 252 Median Pct Recovery = 50% Expected Conc. = 252 Median Pct Recovery = 50% Expected Conc. = 252 Median Pct Recovery = 50% Expected Conc. = 252 Median Pct Recovery = 50% Expected Conc. = 249 Median Pct Recovery = 50% Expected Conc. = 249 Median Pct Recovery = 50% Expected Conc. = 249 Median Pct Recovery = 50% Expected Conc. = 249 Median Pct Recovery = 50% Expected Conc. = 402 Median Pct Recovery = 50% Expected Conc. = 402 Median Pct Recovery = 50% Expected Conc. = 249 Median Pct Recovery = 50% Analysis Date = 11/09/16 SpikeMix = Abs 050916sed3H2: 0 µl & Abs 050916sed3L3: 0 µl Pct Recovery = 50% Analysis Date = 10/12/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 050916sed3H2: 0 µl Pct Recovery = 56% Analysis Date = 03/17/17 SpikeMix = ERA 04121604: 0 µl & ERA 04121605: 0 µl Pct Recovery = 50% Analysis Date = 03/17/17 SpikeMix = ERA 04121605: 0 µl Pct Recovery = 87% Analysis Date = 03/15/17 SpikeMix = ERA 04121605: 0 µl & ERA 04121606: 0 µl Pct Recovery = 46% Analysis Date = 03/15/17 SpikeMix = ERA 04121605: 0 µl & Abs 051816sed3H1: 0 µl Pct Recovery = 48% Analysis Date = 02/10/17 SpikeMix = ERA 04121604: 0 µl & ERA 04121605: 0 µl Pct Recovery = 47% Analysis Date = 02/10/17 SpikeMix = ERA 04121605: 0 µl & ERA 04121606: 0 µl Pct Recovery = 46% Analysis Date = 02/21/17 SpikeMix = ERA 04121604: 0 µl & Abs 050916sed3L2: 0 µl Pct Recovery = 51% Analysis Date = 11/09/16 SpikeMix = Abs 051816sed3L1: 0 µl & Abs 050916sed3L2: 0 µl Pct Recovery = 59% Median Pct Recovery = 50% Median Pct Recovery = 50% Median Pct Recovery = 50% Median Pct Recovery = 50% Median Pct Recovery = 50% Median Pct Recovery = 50% Median Pct Recovery = 50% Median Pct Recovery = 50% Median Pct Recovery = 50% Median Pct Recovery = 50% Median Pct Recovery = 50% Median Pct Recovery = 50% Median Pct Recovery = 50% Median Pct Recovery = 50% Median Pct Recovery = 50% Median Pct Recovery = 50% Median Pct Recovery = 50% Median Pct Recovery = 50% Median Pct Recovery = 50% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
BETA-SITOSTEROL
METHOD: 5433 , TESTIDCODE: 63185GM008
DATES: 10/12/16 - 03/17/17
Open Data Set

Expected Conc. = 4014 Median Pct Recovery = 72% Expected Conc. = 4014 Median Pct Recovery = 72% Expected Conc. = 4014 Median Pct Recovery = 72% Expected Conc. = 2509 Median Pct Recovery = 72% Expected Conc. = 2509 Median Pct Recovery = 72% Expected Conc. = 2509 Median Pct Recovery = 72% Expected Conc. = 2509 Median Pct Recovery = 72% Expected Conc. = 2500 Median Pct Recovery = 72% Expected Conc. = 2500 Median Pct Recovery = 72% Expected Conc. = 2500 Median Pct Recovery = 72% Expected Conc. = 2500 Median Pct Recovery = 72% Expected Conc. = 2500 Median Pct Recovery = 72% Expected Conc. = 2500 Median Pct Recovery = 72% Expected Conc. = 2500 Median Pct Recovery = 72% Expected Conc. = 2500 Median Pct Recovery = 72% Expected Conc. = 2500 Median Pct Recovery = 72% Expected Conc. = 2500 Median Pct Recovery = 72% Expected Conc. = 2500 Median Pct Recovery = 72% Expected Conc. = 2500 Median Pct Recovery = 72% Expected Conc. = 4014 Median Pct Recovery = 72% Expected Conc. = 4014 Median Pct Recovery = 72% Expected Conc. = 2509 Median Pct Recovery = 72% Analysis Date = 11/09/16 SpikeMix = Abs 050916sed3H2: 0 µl & Abs 050916sed3L3: 0 µl Pct Recovery = 74% Analysis Date = 10/12/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 050916sed3H2: 0 µl Pct Recovery = 98% Analysis Date = 02/21/17 SpikeMix = ERA 04121604: 0 µl & Abs 050916sed3L2: 0 µl Pct Recovery = 126% Analysis Date = 11/09/16 SpikeMix = Abs 051816sed3L1: 0 µl & Abs 050916sed3L2: 0 µl Pct Recovery = 115% Analysis Date = 03/17/17 SpikeMix = ERA 04121604: 0 µl & ERA 04121605: 0 µl Pct Recovery = 55% Analysis Date = 03/17/17 SpikeMix = ERA 04121605: 0 µl Pct Recovery = 69% Analysis Date = 03/15/17 SpikeMix = ERA 04121605: 0 µl & ERA 04121606: 0 µl Pct Recovery = 70% Analysis Date = 03/15/17 SpikeMix = ERA 04121605: 0 µl & Abs 051816sed3H1: 0 µl Pct Recovery = 106% Analysis Date = 02/10/17 SpikeMix = ERA 04121604: 0 µl & ERA 04121605: 0 µl Pct Recovery = 52% Analysis Date = 02/10/17 SpikeMix = ERA 04121605: 0 µl & ERA 04121606: 0 µl Pct Recovery = 48% Median Pct Recovery = 72% Median Pct Recovery = 72% Median Pct Recovery = 72% Median Pct Recovery = 72% Median Pct Recovery = 72% Median Pct Recovery = 72% Median Pct Recovery = 72% Median Pct Recovery = 72% Median Pct Recovery = 72% Median Pct Recovery = 72% Median Pct Recovery = 72% Median Pct Recovery = 72% Median Pct Recovery = 72% Median Pct Recovery = 72% Median Pct Recovery = 72% Median Pct Recovery = 72% Median Pct Recovery = 72% Median Pct Recovery = 72% Median Pct Recovery = 72% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
BETA-STIGMASTANOL
METHOD: 5433 , TESTIDCODE: 63186GM008
DATES: 11/09/16 - 03/17/17
Open Data Set

Expected Conc. = 4005 Median Pct Recovery = 42% Expected Conc. = 4005 Median Pct Recovery = 42% Expected Conc. = 4005 Median Pct Recovery = 42% Expected Conc. = 2508 Median Pct Recovery = 42% Expected Conc. = 2508 Median Pct Recovery = 42% Expected Conc. = 2508 Median Pct Recovery = 42% Expected Conc. = 2508 Median Pct Recovery = 42% Expected Conc. = 2500 Median Pct Recovery = 42% Expected Conc. = 2500 Median Pct Recovery = 42% Expected Conc. = 2500 Median Pct Recovery = 42% Expected Conc. = 2500 Median Pct Recovery = 42% Expected Conc. = 2500 Median Pct Recovery = 42% Expected Conc. = 2500 Median Pct Recovery = 42% Expected Conc. = 2500 Median Pct Recovery = 42% Expected Conc. = 2500 Median Pct Recovery = 42% Expected Conc. = 2500 Median Pct Recovery = 42% Expected Conc. = 2500 Median Pct Recovery = 42% Expected Conc. = 2500 Median Pct Recovery = 42% Expected Conc. = 2500 Median Pct Recovery = 42% Expected Conc. = 4005 Median Pct Recovery = 42% Expected Conc. = 4005 Median Pct Recovery = 42% Expected Conc. = 2508 Median Pct Recovery = 42% Analysis Date = 03/15/17 SpikeMix = ERA 04121605: 0 µl & Abs 051816sed3H1: 0 µl Pct Recovery = 56% Analysis Date = 11/10/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 051816sed3H1: 0 µl Pct Recovery = 27% Analysis Date = 11/09/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 051816sed3L1: 0 µl Pct Recovery = 42% Analysis Date = 11/09/16 SpikeMix = Abs 051816sed3L1: 0 µl & Abs 050916sed3L2: 0 µl Pct Recovery = 47% Analysis Date = 03/17/17 SpikeMix = Abs 050916sed3L3: 0 µl & ERA 04121604: 0 µl Pct Recovery = 41% Analysis Date = 03/17/17 SpikeMix = ERA 04121604: 0 µl & ERA 04121605: 0 µl Pct Recovery = 35% Analysis Date = 03/17/17 SpikeMix = ERA 04121606: 0 µl & ERA 04121604: 0 µl Pct Recovery = 30% Analysis Date = 02/21/17 SpikeMix = ERA 04121606: 0 µl & ERA 04121604: 0 µl Pct Recovery = 45% Analysis Date = 02/21/17 SpikeMix = ERA 04121604: 0 µl & Abs 050916sed3L2: 0 µl Pct Recovery = 60% Analysis Date = 02/10/17 SpikeMix = ERA 04121604: 0 µl & ERA 04121605: 0 µl Pct Recovery = 31% Median Pct Recovery = 42% Median Pct Recovery = 42% Median Pct Recovery = 42% Median Pct Recovery = 42% Median Pct Recovery = 42% Median Pct Recovery = 42% Median Pct Recovery = 42% Median Pct Recovery = 42% Median Pct Recovery = 42% Median Pct Recovery = 42% Median Pct Recovery = 42% Median Pct Recovery = 42% Median Pct Recovery = 42% Median Pct Recovery = 42% Median Pct Recovery = 42% Median Pct Recovery = 42% Median Pct Recovery = 42% Median Pct Recovery = 42% Median Pct Recovery = 42% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
BIS(2-ETHYLHEXYL) PHTHALATE
METHOD: 5433 , TESTIDCODE: 63187GM008
DATES: 10/12/16 - 03/17/17
Open Data Set

Expected Conc. = 2012 Median Pct Recovery = 44% Expected Conc. = 2012 Median Pct Recovery = 44% Expected Conc. = 2012 Median Pct Recovery = 44% Expected Conc. = 2012 Median Pct Recovery = 44% Expected Conc. = 2012 Median Pct Recovery = 44% Expected Conc. = 1251 Median Pct Recovery = 44% Expected Conc. = 1251 Median Pct Recovery = 44% Expected Conc. = 1251 Median Pct Recovery = 44% Expected Conc. = 1251 Median Pct Recovery = 44% Expected Conc. = 1240 Median Pct Recovery = 44% Expected Conc. = 1240 Median Pct Recovery = 44% Expected Conc. = 1240 Median Pct Recovery = 44% Expected Conc. = 1240 Median Pct Recovery = 44% Expected Conc. = 1240 Median Pct Recovery = 44% Expected Conc. = 1240 Median Pct Recovery = 44% Expected Conc. = 1240 Median Pct Recovery = 44% Expected Conc. = 1240 Median Pct Recovery = 44% Expected Conc. = 1240 Median Pct Recovery = 44% Expected Conc. = 1240 Median Pct Recovery = 44% Expected Conc. = 1251 Median Pct Recovery = 44% Expected Conc. = 1251 Median Pct Recovery = 44% Expected Conc. = 1240 Median Pct Recovery = 44% Analysis Date = 11/10/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 051816sed3H1: 0 µl Pct Recovery = 26% Analysis Date = 11/09/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 051816sed3L1: 0 µl Pct Recovery = 41% Analysis Date = 10/12/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 050916sed3H2: 0 µl Pct Recovery = 45% Analysis Date = 03/17/17 SpikeMix = Abs 050916sed3L3: 0 µl & ERA 04121604: 0 µl Pct Recovery = 46% Analysis Date = 11/09/16 SpikeMix = Abs 050916sed3H2: 0 µl & Abs 050916sed3L3: 0 µl Pct Recovery = 46% Analysis Date = 03/17/17 SpikeMix = ERA 04121606: 0 µl Pct Recovery = 85% Analysis Date = 03/17/17 SpikeMix = ERA 04121606: 0 µl & ERA 04121604: 0 µl Pct Recovery = 36% Analysis Date = 03/15/17 SpikeMix = ERA 04121605: 0 µl & ERA 04121606: 0 µl Pct Recovery = 38% Analysis Date = 02/21/17 SpikeMix = ERA 04121606: 0 µl & ERA 04121604: 0 µl Pct Recovery = 45% Analysis Date = 02/10/17 SpikeMix = ERA 04121605: 0 µl & ERA 04121606: 0 µl Pct Recovery = 42% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
BISPHENOL A
METHOD: 5433 , TESTIDCODE: 63188GM008
DATES: 10/12/16 - 03/17/17
Open Data Set

Expected Conc. = 401 Median Pct Recovery = 30% Expected Conc. = 401 Median Pct Recovery = 30% Expected Conc. = 401 Median Pct Recovery = 30% Expected Conc. = 401 Median Pct Recovery = 30% Expected Conc. = 401 Median Pct Recovery = 30% Expected Conc. = 250 Median Pct Recovery = 30% Expected Conc. = 250 Median Pct Recovery = 30% Expected Conc. = 250 Median Pct Recovery = 30% Expected Conc. = 250 Median Pct Recovery = 30% Expected Conc. = 250 Median Pct Recovery = 30% Expected Conc. = 250 Median Pct Recovery = 30% Expected Conc. = 250 Median Pct Recovery = 30% Expected Conc. = 250 Median Pct Recovery = 30% Expected Conc. = 250 Median Pct Recovery = 30% Expected Conc. = 250 Median Pct Recovery = 30% Expected Conc. = 248 Median Pct Recovery = 30% Expected Conc. = 248 Median Pct Recovery = 30% Expected Conc. = 248 Median Pct Recovery = 30% Expected Conc. = 248 Median Pct Recovery = 30% Expected Conc. = 250 Median Pct Recovery = 30% Expected Conc. = 250 Median Pct Recovery = 30% Expected Conc. = 248 Median Pct Recovery = 30% Analysis Date = 11/10/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 051816sed3H1: 0 µl Pct Recovery = 24% Analysis Date = 11/09/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 051816sed3L1: 0 µl Pct Recovery = 34% Analysis Date = 10/12/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 050916sed3H2: 0 µl Pct Recovery = 41% Analysis Date = 03/17/17 SpikeMix = ERA 04121606: 0 µl Pct Recovery = 26% Analysis Date = 03/17/17 SpikeMix = ERA 04121606: 0 µl & ERA 04121604: 0 µl Pct Recovery = 18% Analysis Date = 03/15/17 SpikeMix = ERA 04121605: 0 µl & ERA 04121606: 0 µl Pct Recovery = 24% Analysis Date = 02/21/17 SpikeMix = ERA 04121606: 0 µl & ERA 04121604: 0 µl Pct Recovery = 33% Analysis Date = 02/10/17 SpikeMix = ERA 04121605: 0 µl & ERA 04121606: 0 µl Pct Recovery = 59% Analysis Date = 03/17/17 SpikeMix = Abs 050916sed3L3: 0 µl & ERA 04121604: 0 µl Pct Recovery = 26% Analysis Date = 11/09/16 SpikeMix = Abs 050916sed3H2: 0 µl & Abs 050916sed3L3: 0 µl Pct Recovery = 34% Median Pct Recovery = 30% Median Pct Recovery = 30% Median Pct Recovery = 30% Median Pct Recovery = 30% Median Pct Recovery = 30% Median Pct Recovery = 30% Median Pct Recovery = 30% Median Pct Recovery = 30% Median Pct Recovery = 30% Median Pct Recovery = 30% Median Pct Recovery = 30% Median Pct Recovery = 30% Median Pct Recovery = 30% Median Pct Recovery = 30% Median Pct Recovery = 30% Median Pct Recovery = 30% Median Pct Recovery = 30% Median Pct Recovery = 30% Median Pct Recovery = 30% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
BROMACIL
METHOD: 5433 , TESTIDCODE: 63189GM008
DATES: 11/09/16 - 03/17/17
Open Data Set

Expected Conc. = 4004 Median Pct Recovery = 33% Expected Conc. = 4004 Median Pct Recovery = 33% Expected Conc. = 4004 Median Pct Recovery = 33% Expected Conc. = 2510 Median Pct Recovery = 33% Expected Conc. = 2510 Median Pct Recovery = 33% Expected Conc. = 2510 Median Pct Recovery = 33% Expected Conc. = 2510 Median Pct Recovery = 33% Expected Conc. = 2510 Median Pct Recovery = 33% Expected Conc. = 2510 Median Pct Recovery = 33% Expected Conc. = 2510 Median Pct Recovery = 33% Expected Conc. = 2510 Median Pct Recovery = 33% Expected Conc. = 2510 Median Pct Recovery = 33% Expected Conc. = 2510 Median Pct Recovery = 33% Expected Conc. = 2510 Median Pct Recovery = 33% Expected Conc. = 2510 Median Pct Recovery = 33% Expected Conc. = 2507 Median Pct Recovery = 33% Expected Conc. = 2507 Median Pct Recovery = 33% Expected Conc. = 2507 Median Pct Recovery = 33% Expected Conc. = 2507 Median Pct Recovery = 33% Expected Conc. = 4004 Median Pct Recovery = 33% Expected Conc. = 4004 Median Pct Recovery = 33% Expected Conc. = 2507 Median Pct Recovery = 33% Analysis Date = 03/15/17 SpikeMix = ERA 04121605: 0 µl & Abs 051816sed3H1: 0 µl Pct Recovery = 30% Analysis Date = 11/10/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 051816sed3H1: 0 µl Pct Recovery = 14% Analysis Date = 03/17/17 SpikeMix = Abs 050916sed3L3: 0 µl & ERA 04121604: 0 µl Pct Recovery = 18% Analysis Date = 03/17/17 SpikeMix = ERA 04121604: 0 µl & ERA 04121605: 0 µl Pct Recovery = 37% Analysis Date = 03/17/17 SpikeMix = ERA 04121606: 0 µl & ERA 04121604: 0 µl Pct Recovery = 36% Analysis Date = 02/21/17 SpikeMix = ERA 04121606: 0 µl & ERA 04121604: 0 µl Pct Recovery = 41% Analysis Date = 02/21/17 SpikeMix = ERA 04121604: 0 µl & Abs 050916sed3L2: 0 µl Pct Recovery = 37% Analysis Date = 02/10/17 SpikeMix = ERA 04121604: 0 µl & ERA 04121605: 0 µl Pct Recovery = 40% Analysis Date = 11/09/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 051816sed3L1: 0 µl Pct Recovery = 20% Analysis Date = 11/09/16 SpikeMix = Abs 051816sed3L1: 0 µl & Abs 050916sed3L2: 0 µl Pct Recovery = 22% Median Pct Recovery = 33% Median Pct Recovery = 33% Median Pct Recovery = 33% Median Pct Recovery = 33% Median Pct Recovery = 33% Median Pct Recovery = 33% Median Pct Recovery = 33% Median Pct Recovery = 33% Median Pct Recovery = 33% Median Pct Recovery = 33% Median Pct Recovery = 33% Median Pct Recovery = 33% Median Pct Recovery = 33% Median Pct Recovery = 33% Median Pct Recovery = 33% Median Pct Recovery = 33% Median Pct Recovery = 33% Median Pct Recovery = 33% Median Pct Recovery = 33% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
CAMPHOR
METHOD: 5433 , TESTIDCODE: 63192GM008
DATES: 10/12/16 - 03/17/17
Open Data Set

Expected Conc. = 401 Median Pct Recovery = 32% Expected Conc. = 401 Median Pct Recovery = 32% Expected Conc. = 401 Median Pct Recovery = 32% Expected Conc. = 253 Median Pct Recovery = 32% Expected Conc. = 253 Median Pct Recovery = 32% Expected Conc. = 253 Median Pct Recovery = 32% Expected Conc. = 253 Median Pct Recovery = 32% Expected Conc. = 253 Median Pct Recovery = 32% Expected Conc. = 253 Median Pct Recovery = 32% Expected Conc. = 253 Median Pct Recovery = 32% Expected Conc. = 253 Median Pct Recovery = 32% Expected Conc. = 253 Median Pct Recovery = 32% Expected Conc. = 253 Median Pct Recovery = 32% Expected Conc. = 253 Median Pct Recovery = 32% Expected Conc. = 253 Median Pct Recovery = 32% Expected Conc. = 249 Median Pct Recovery = 32% Expected Conc. = 249 Median Pct Recovery = 32% Expected Conc. = 249 Median Pct Recovery = 32% Expected Conc. = 249 Median Pct Recovery = 32% Expected Conc. = 401 Median Pct Recovery = 32% Expected Conc. = 401 Median Pct Recovery = 32% Expected Conc. = 249 Median Pct Recovery = 32% Analysis Date = 11/09/16 SpikeMix = Abs 050916sed3H2: 0 µl & Abs 050916sed3L3: 0 µl Pct Recovery = 16% Analysis Date = 10/12/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 050916sed3H2: 0 µl Pct Recovery = 24% Analysis Date = 03/17/17 SpikeMix = ERA 04121604: 0 µl & ERA 04121605: 0 µl Pct Recovery = 34% Analysis Date = 03/17/17 SpikeMix = ERA 04121605: 0 µl Pct Recovery = 68% Analysis Date = 03/15/17 SpikeMix = ERA 04121605: 0 µl & ERA 04121606: 0 µl Pct Recovery = 34% Analysis Date = 03/15/17 SpikeMix = ERA 04121605: 0 µl & Abs 051816sed3H1: 0 µl Pct Recovery = 30% Analysis Date = 02/10/17 SpikeMix = ERA 04121604: 0 µl & ERA 04121605: 0 µl Pct Recovery = 34% Analysis Date = 02/10/17 SpikeMix = ERA 04121605: 0 µl & ERA 04121606: 0 µl Pct Recovery = 37% Analysis Date = 02/21/17 SpikeMix = ERA 04121604: 0 µl & Abs 050916sed3L2: 0 µl Pct Recovery = 19% Analysis Date = 11/09/16 SpikeMix = Abs 051816sed3L1: 0 µl & Abs 050916sed3L2: 0 µl Pct Recovery = 23% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
CARBAZOLE
METHOD: 5433 , TESTIDCODE: 63194GM008
DATES: 11/09/16 - 03/17/17
Open Data Set

Expected Conc. = 401 Median Pct Recovery = 39% Expected Conc. = 401 Median Pct Recovery = 39% Expected Conc. = 401 Median Pct Recovery = 39% Expected Conc. = 257 Median Pct Recovery = 39% Expected Conc. = 257 Median Pct Recovery = 39% Expected Conc. = 257 Median Pct Recovery = 39% Expected Conc. = 257 Median Pct Recovery = 39% Expected Conc. = 251 Median Pct Recovery = 39% Expected Conc. = 251 Median Pct Recovery = 39% Expected Conc. = 251 Median Pct Recovery = 39% Expected Conc. = 251 Median Pct Recovery = 39% Expected Conc. = 251 Median Pct Recovery = 39% Expected Conc. = 251 Median Pct Recovery = 39% Expected Conc. = 251 Median Pct Recovery = 39% Expected Conc. = 251 Median Pct Recovery = 39% Expected Conc. = 251 Median Pct Recovery = 39% Expected Conc. = 251 Median Pct Recovery = 39% Expected Conc. = 251 Median Pct Recovery = 39% Expected Conc. = 251 Median Pct Recovery = 39% Expected Conc. = 401 Median Pct Recovery = 39% Expected Conc. = 401 Median Pct Recovery = 39% Expected Conc. = 257 Median Pct Recovery = 39% Analysis Date = 03/15/17 SpikeMix = ERA 04121605: 0 µl & Abs 051816sed3H1: 0 µl Pct Recovery = 37% Analysis Date = 11/10/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 051816sed3H1: 0 µl Pct Recovery = 108% Analysis Date = 11/09/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 051816sed3L1: 0 µl Pct Recovery = 40% Analysis Date = 11/09/16 SpikeMix = Abs 051816sed3L1: 0 µl & Abs 050916sed3L2: 0 µl Pct Recovery = 39% Analysis Date = 03/17/17 SpikeMix = Abs 050916sed3L3: 0 µl & ERA 04121604: 0 µl Pct Recovery = 37% Analysis Date = 03/17/17 SpikeMix = ERA 04121604: 0 µl & ERA 04121605: 0 µl Pct Recovery = 37% Analysis Date = 03/17/17 SpikeMix = ERA 04121606: 0 µl & ERA 04121604: 0 µl Pct Recovery = 34% Analysis Date = 02/21/17 SpikeMix = ERA 04121606: 0 µl & ERA 04121604: 0 µl Pct Recovery = 39% Analysis Date = 02/21/17 SpikeMix = ERA 04121604: 0 µl & Abs 050916sed3L2: 0 µl Pct Recovery = 43% Analysis Date = 02/10/17 SpikeMix = ERA 04121604: 0 µl & ERA 04121605: 0 µl Pct Recovery = 42% Median Pct Recovery = 39% Median Pct Recovery = 39% Median Pct Recovery = 39% Median Pct Recovery = 39% Median Pct Recovery = 39% Median Pct Recovery = 39% Median Pct Recovery = 39% Median Pct Recovery = 39% Median Pct Recovery = 39% Median Pct Recovery = 39% Median Pct Recovery = 39% Median Pct Recovery = 39% Median Pct Recovery = 39% Median Pct Recovery = 39% Median Pct Recovery = 39% Median Pct Recovery = 39% Median Pct Recovery = 39% Median Pct Recovery = 39% Median Pct Recovery = 39% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
CHLORPYRIFOS
METHOD: 5433 , TESTIDCODE: 63195GM008
DATES: 11/09/16 - 03/17/17
Open Data Set

Expected Conc. = 401 Median Pct Recovery = 21% Expected Conc. = 250 Median Pct Recovery = 21% Expected Conc. = 250 Median Pct Recovery = 21% Expected Conc. = 250 Median Pct Recovery = 21% Expected Conc. = 250 Median Pct Recovery = 21% Expected Conc. = 250 Median Pct Recovery = 21% Expected Conc. = 250 Median Pct Recovery = 21% Expected Conc. = 250 Median Pct Recovery = 21% Expected Conc. = 250 Median Pct Recovery = 21% Expected Conc. = 250 Median Pct Recovery = 21% Expected Conc. = 250 Median Pct Recovery = 21% Expected Conc. = 250 Median Pct Recovery = 21% Expected Conc. = 250 Median Pct Recovery = 21% Expected Conc. = 249 Median Pct Recovery = 21% Expected Conc. = 249 Median Pct Recovery = 21% Expected Conc. = 249 Median Pct Recovery = 21% Expected Conc. = 249 Median Pct Recovery = 21% Expected Conc. = 401 Median Pct Recovery = 21% Expected Conc. = 401 Median Pct Recovery = 21% Expected Conc. = 401 Median Pct Recovery = 21% Expected Conc. = 401 Median Pct Recovery = 21% Expected Conc. = 249 Median Pct Recovery = 21% Analysis Date = 03/15/17 SpikeMix = ERA 04121605: 0 µl & Abs 051816sed3H1: 0 µl Pct Recovery = 15% Analysis Date = 03/17/17 SpikeMix = Abs 050916sed3L3: 0 µl & ERA 04121604: 0 µl Pct Recovery = 11% Analysis Date = 03/17/17 SpikeMix = ERA 04121604: 0 µl & ERA 04121605: 0 µl Pct Recovery = 21% Analysis Date = 03/17/17 SpikeMix = ERA 04121606: 0 µl & ERA 04121604: 0 µl Pct Recovery = 21% Analysis Date = 02/21/17 SpikeMix = ERA 04121606: 0 µl & ERA 04121604: 0 µl Pct Recovery = 24% Analysis Date = 02/21/17 SpikeMix = ERA 04121604: 0 µl & Abs 050916sed3L2: 0 µl Pct Recovery = 21% Analysis Date = 02/10/17 SpikeMix = ERA 04121604: 0 µl & ERA 04121605: 0 µl Pct Recovery = 23% Analysis Date = 11/09/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 051816sed3L1: 0 µl Pct Recovery = 18% Analysis Date = 11/09/16 SpikeMix = Abs 051816sed3L1: 0 µl & Abs 050916sed3L2: 0 µl Pct Recovery = 20% Median Pct Recovery = 21% Median Pct Recovery = 21% Median Pct Recovery = 21% Median Pct Recovery = 21% Median Pct Recovery = 21% Median Pct Recovery = 21% Median Pct Recovery = 21% Median Pct Recovery = 21% Median Pct Recovery = 21% Median Pct Recovery = 21% Median Pct Recovery = 21% Median Pct Recovery = 21% Median Pct Recovery = 21% Median Pct Recovery = 21% Median Pct Recovery = 21% Median Pct Recovery = 21% Median Pct Recovery = 21% Median Pct Recovery = 21% Median Pct Recovery = 21% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
CHOLESTEROL
METHOD: 5433 , TESTIDCODE: 63196GM008
DATES: 11/09/16 - 03/17/17
Open Data Set

Expected Conc. = 2012 Median Pct Recovery = 56% Expected Conc. = 2012 Median Pct Recovery = 56% Expected Conc. = 2012 Median Pct Recovery = 56% Expected Conc. = 1259 Median Pct Recovery = 56% Expected Conc. = 1259 Median Pct Recovery = 56% Expected Conc. = 1259 Median Pct Recovery = 56% Expected Conc. = 1259 Median Pct Recovery = 56% Expected Conc. = 1250 Median Pct Recovery = 56% Expected Conc. = 1250 Median Pct Recovery = 56% Expected Conc. = 1250 Median Pct Recovery = 56% Expected Conc. = 1250 Median Pct Recovery = 56% Expected Conc. = 1250 Median Pct Recovery = 56% Expected Conc. = 1250 Median Pct Recovery = 56% Expected Conc. = 1250 Median Pct Recovery = 56% Expected Conc. = 1250 Median Pct Recovery = 56% Expected Conc. = 2012 Median Pct Recovery = 56% Expected Conc. = 2012 Median Pct Recovery = 56% Expected Conc. = 1259 Median Pct Recovery = 56% Expected Conc. = 1259 Median Pct Recovery = 56% Expected Conc. = 1250 Median Pct Recovery = 56% Expected Conc. = 1250 Median Pct Recovery = 56% Expected Conc. = 1250 Median Pct Recovery = 56% Analysis Date = 03/15/17 SpikeMix = ERA 04121605: 0 µl & Abs 051816sed3H1: 0 µl Pct Recovery = 57% Analysis Date = 11/10/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 051816sed3H1: 0 µl Pct Recovery = 42% Analysis Date = 11/09/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 051816sed3L1: 0 µl Pct Recovery = 59% Analysis Date = 11/09/16 SpikeMix = Abs 051816sed3L1: 0 µl & Abs 050916sed3L2: 0 µl Pct Recovery = 53% Analysis Date = 03/17/17 SpikeMix = Abs 050916sed3L3: 0 µl & ERA 04121604: 0 µl Pct Recovery = 66% Analysis Date = 02/21/17 SpikeMix = ERA 04121606: 0 µl & ERA 04121604: 0 µl Pct Recovery = 55% Analysis Date = 02/21/17 SpikeMix = ERA 04121604: 0 µl & Abs 050916sed3L2: 0 µl Pct Recovery = 63% Analysis Date = 02/10/17 SpikeMix = ERA 04121604: 0 µl & ERA 04121605: 0 µl Pct Recovery = 44% Median Pct Recovery = 56% Median Pct Recovery = 56% Median Pct Recovery = 56% Median Pct Recovery = 56% Median Pct Recovery = 56% Median Pct Recovery = 56% Median Pct Recovery = 56% Median Pct Recovery = 56% Median Pct Recovery = 56% Median Pct Recovery = 56% Median Pct Recovery = 56% Median Pct Recovery = 56% Median Pct Recovery = 56% Median Pct Recovery = 56% Median Pct Recovery = 56% Median Pct Recovery = 56% Median Pct Recovery = 56% Median Pct Recovery = 56% Median Pct Recovery = 56% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
DIAZINON
METHOD: 5433 , TESTIDCODE: 63198GM008
DATES: 10/12/16 - 03/17/17
Open Data Set

Expected Conc. = 401 Median Pct Recovery = 28% Expected Conc. = 401 Median Pct Recovery = 28% Expected Conc. = 401 Median Pct Recovery = 28% Expected Conc. = 252 Median Pct Recovery = 28% Expected Conc. = 252 Median Pct Recovery = 28% Expected Conc. = 252 Median Pct Recovery = 28% Expected Conc. = 252 Median Pct Recovery = 28% Expected Conc. = 252 Median Pct Recovery = 28% Expected Conc. = 252 Median Pct Recovery = 28% Expected Conc. = 252 Median Pct Recovery = 28% Expected Conc. = 252 Median Pct Recovery = 28% Expected Conc. = 252 Median Pct Recovery = 28% Expected Conc. = 252 Median Pct Recovery = 28% Expected Conc. = 252 Median Pct Recovery = 28% Expected Conc. = 252 Median Pct Recovery = 28% Expected Conc. = 249 Median Pct Recovery = 28% Expected Conc. = 249 Median Pct Recovery = 28% Expected Conc. = 249 Median Pct Recovery = 28% Expected Conc. = 249 Median Pct Recovery = 28% Expected Conc. = 401 Median Pct Recovery = 28% Expected Conc. = 401 Median Pct Recovery = 28% Expected Conc. = 249 Median Pct Recovery = 28% Analysis Date = 11/09/16 SpikeMix = Abs 050916sed3H2: 0 µl & Abs 050916sed3L3: 0 µl Pct Recovery = 11% Analysis Date = 10/12/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 050916sed3H2: 0 µl Pct Recovery = 24% Analysis Date = 03/17/17 SpikeMix = ERA 04121604: 0 µl & ERA 04121605: 0 µl Pct Recovery = 35% Analysis Date = 03/17/17 SpikeMix = ERA 04121605: 0 µl Pct Recovery = 70% Analysis Date = 03/15/17 SpikeMix = ERA 04121605: 0 µl & ERA 04121606: 0 µl Pct Recovery = 32% Analysis Date = 03/15/17 SpikeMix = ERA 04121605: 0 µl & Abs 051816sed3H1: 0 µl Pct Recovery = 22% Analysis Date = 02/10/17 SpikeMix = ERA 04121604: 0 µl & ERA 04121605: 0 µl Pct Recovery = 34% Analysis Date = 02/10/17 SpikeMix = ERA 04121605: 0 µl & ERA 04121606: 0 µl Pct Recovery = 32% Analysis Date = 02/21/17 SpikeMix = ERA 04121604: 0 µl & Abs 050916sed3L2: 0 µl Pct Recovery = 17% Analysis Date = 11/09/16 SpikeMix = Abs 051816sed3L1: 0 µl & Abs 050916sed3L2: 0 µl Pct Recovery = 18% Median Pct Recovery = 28% Median Pct Recovery = 28% Median Pct Recovery = 28% Median Pct Recovery = 28% Median Pct Recovery = 28% Median Pct Recovery = 28% Median Pct Recovery = 28% Median Pct Recovery = 28% Median Pct Recovery = 28% Median Pct Recovery = 28% Median Pct Recovery = 28% Median Pct Recovery = 28% Median Pct Recovery = 28% Median Pct Recovery = 28% Median Pct Recovery = 28% Median Pct Recovery = 28% Median Pct Recovery = 28% Median Pct Recovery = 28% Median Pct Recovery = 28% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
DIETHYL PHTHALATE
METHOD: 5433 , TESTIDCODE: 63202GM008
DATES: 10/12/16 - 11/10/16
Open Data Set

Expected Conc. = 800 Median Pct Recovery = 38% Expected Conc. = 800 Median Pct Recovery = 38% Expected Conc. = 800 Median Pct Recovery = 38% Expected Conc. = 800 Median Pct Recovery = 38% Expected Conc. = 800 Median Pct Recovery = 38% Expected Conc. = 507 Median Pct Recovery = 38% Expected Conc. = 507 Median Pct Recovery = 38% Expected Conc. = 507 Median Pct Recovery = 38% Expected Conc. = 507 Median Pct Recovery = 38% Expected Conc. = 507 Median Pct Recovery = 38% Expected Conc. = 507 Median Pct Recovery = 38% Expected Conc. = 501 Median Pct Recovery = 38% Expected Conc. = 501 Median Pct Recovery = 38% Expected Conc. = 501 Median Pct Recovery = 38% Expected Conc. = 501 Median Pct Recovery = 38% Expected Conc. = 501 Median Pct Recovery = 38% Expected Conc. = 501 Median Pct Recovery = 38% Expected Conc. = 501 Median Pct Recovery = 38% Expected Conc. = 501 Median Pct Recovery = 38% Expected Conc. = 501 Median Pct Recovery = 38% Expected Conc. = 501 Median Pct Recovery = 38% Expected Conc. = 501 Median Pct Recovery = 38% Analysis Date = 11/10/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 051816sed3H1: 0 µl Pct Recovery = 17% Analysis Date = 11/09/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 051816sed3L1: 0 µl Pct Recovery = 36% Analysis Date = 10/12/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 050916sed3H2: 0 µl Pct Recovery = 40% Analysis Date = 11/09/16 SpikeMix = Abs 050916sed3H2: 0 µl & Abs 050916sed3L3: 0 µl Pct Recovery = 39% Median Pct Recovery = 38% Median Pct Recovery = 38% Median Pct Recovery = 38% Median Pct Recovery = 38% Median Pct Recovery = 38% Median Pct Recovery = 38% Median Pct Recovery = 38% Median Pct Recovery = 38% Median Pct Recovery = 38% Median Pct Recovery = 38% Median Pct Recovery = 38% Median Pct Recovery = 38% Median Pct Recovery = 38% Median Pct Recovery = 38% Median Pct Recovery = 38% Median Pct Recovery = 38% Median Pct Recovery = 38% Median Pct Recovery = 38% Median Pct Recovery = 38% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
D-LIMONENE
METHOD: 5433 , TESTIDCODE: 63203GM008
DATES: 10/12/16 - 03/17/17
Open Data Set

Expected Conc. = 401 Median Pct Recovery = 16% Expected Conc. = 249 Median Pct Recovery = 16% Expected Conc. = 249 Median Pct Recovery = 16% Expected Conc. = 249 Median Pct Recovery = 16% Expected Conc. = 249 Median Pct Recovery = 16% Expected Conc. = 249 Median Pct Recovery = 16% Expected Conc. = 249 Median Pct Recovery = 16% Expected Conc. = 249 Median Pct Recovery = 16% Expected Conc. = 249 Median Pct Recovery = 16% Expected Conc. = 249 Median Pct Recovery = 16% Expected Conc. = 249 Median Pct Recovery = 16% Expected Conc. = 401 Median Pct Recovery = 16% Expected Conc. = 401 Median Pct Recovery = 16% Expected Conc. = 401 Median Pct Recovery = 16% Expected Conc. = 401 Median Pct Recovery = 16% Expected Conc. = 249 Median Pct Recovery = 16% Expected Conc. = 249 Median Pct Recovery = 16% Expected Conc. = 249 Median Pct Recovery = 16% Expected Conc. = 249 Median Pct Recovery = 16% Expected Conc. = 249 Median Pct Recovery = 16% Expected Conc. = 249 Median Pct Recovery = 16% Expected Conc. = 249 Median Pct Recovery = 16% Analysis Date = 10/12/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 050916sed3H2: 0 µl Pct Recovery = 11% Analysis Date = 03/17/17 SpikeMix = ERA 04121604: 0 µl & ERA 04121605: 0 µl Pct Recovery = 18% Analysis Date = 03/17/17 SpikeMix = ERA 04121605: 0 µl Pct Recovery = 33% Analysis Date = 03/15/17 SpikeMix = ERA 04121605: 0 µl & ERA 04121606: 0 µl Pct Recovery = 11% Analysis Date = 02/10/17 SpikeMix = ERA 04121604: 0 µl & ERA 04121605: 0 µl Pct Recovery = 16% Analysis Date = 02/10/17 SpikeMix = ERA 04121605: 0 µl & ERA 04121606: 0 µl Pct Recovery = 15% Median Pct Recovery = 16% Median Pct Recovery = 16% Median Pct Recovery = 16% Median Pct Recovery = 16% Median Pct Recovery = 16% Median Pct Recovery = 16% Median Pct Recovery = 16% Median Pct Recovery = 16% Median Pct Recovery = 16% Median Pct Recovery = 16% Median Pct Recovery = 16% Median Pct Recovery = 16% Median Pct Recovery = 16% Median Pct Recovery = 16% Median Pct Recovery = 16% Median Pct Recovery = 16% Median Pct Recovery = 16% Median Pct Recovery = 16% Median Pct Recovery = 16% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
4-OCTYLPHENOL MONOETHOXYLATES
METHOD: 5433 , TESTIDCODE: 63206GM008
DATES: 11/09/16 - 03/17/17
Open Data Set

Expected Conc. = 2005 Median Pct Recovery = 44% Expected Conc. = 2005 Median Pct Recovery = 44% Expected Conc. = 2005 Median Pct Recovery = 44% Expected Conc. = 1257 Median Pct Recovery = 44% Expected Conc. = 1257 Median Pct Recovery = 44% Expected Conc. = 1257 Median Pct Recovery = 44% Expected Conc. = 1257 Median Pct Recovery = 44% Expected Conc. = 1250 Median Pct Recovery = 44% Expected Conc. = 1250 Median Pct Recovery = 44% Expected Conc. = 1250 Median Pct Recovery = 44% Expected Conc. = 1250 Median Pct Recovery = 44% Expected Conc. = 1250 Median Pct Recovery = 44% Expected Conc. = 1250 Median Pct Recovery = 44% Expected Conc. = 1250 Median Pct Recovery = 44% Expected Conc. = 1250 Median Pct Recovery = 44% Expected Conc. = 1250 Median Pct Recovery = 44% Expected Conc. = 1250 Median Pct Recovery = 44% Expected Conc. = 1250 Median Pct Recovery = 44% Expected Conc. = 1250 Median Pct Recovery = 44% Expected Conc. = 2005 Median Pct Recovery = 44% Expected Conc. = 2005 Median Pct Recovery = 44% Expected Conc. = 1257 Median Pct Recovery = 44% Analysis Date = 03/15/17 SpikeMix = ERA 04121605: 0 µl & Abs 051816sed3H1: 0 µl Pct Recovery = 47% Analysis Date = 11/10/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 051816sed3H1: 0 µl Pct Recovery = 28% Analysis Date = 11/09/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 051816sed3L1: 0 µl Pct Recovery = 44% Analysis Date = 11/09/16 SpikeMix = Abs 051816sed3L1: 0 µl & Abs 050916sed3L2: 0 µl Pct Recovery = 46% Analysis Date = 03/17/17 SpikeMix = Abs 050916sed3L3: 0 µl & ERA 04121604: 0 µl Pct Recovery = 39% Analysis Date = 03/17/17 SpikeMix = ERA 04121604: 0 µl & ERA 04121605: 0 µl Pct Recovery = 38% Analysis Date = 03/17/17 SpikeMix = ERA 04121606: 0 µl & ERA 04121604: 0 µl Pct Recovery = 35% Analysis Date = 02/21/17 SpikeMix = ERA 04121606: 0 µl & ERA 04121604: 0 µl Pct Recovery = 47% Analysis Date = 02/21/17 SpikeMix = ERA 04121604: 0 µl & Abs 050916sed3L2: 0 µl Pct Recovery = 53% Analysis Date = 02/10/17 SpikeMix = ERA 04121604: 0 µl & ERA 04121605: 0 µl Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
FLUORANTHENE
METHOD: 5433 , TESTIDCODE: 63208GM008
DATES: 11/09/16 - 03/17/17
Open Data Set

Expected Conc. = 401 Median Pct Recovery = 50% Expected Conc. = 401 Median Pct Recovery = 50% Expected Conc. = 401 Median Pct Recovery = 50% Expected Conc. = 251 Median Pct Recovery = 50% Expected Conc. = 251 Median Pct Recovery = 50% Expected Conc. = 251 Median Pct Recovery = 50% Expected Conc. = 251 Median Pct Recovery = 50% Expected Conc. = 251 Median Pct Recovery = 50% Expected Conc. = 251 Median Pct Recovery = 50% Expected Conc. = 251 Median Pct Recovery = 50% Expected Conc. = 251 Median Pct Recovery = 50% Expected Conc. = 251 Median Pct Recovery = 50% Expected Conc. = 251 Median Pct Recovery = 50% Expected Conc. = 251 Median Pct Recovery = 50% Expected Conc. = 251 Median Pct Recovery = 50% Expected Conc. = 248 Median Pct Recovery = 50% Expected Conc. = 248 Median Pct Recovery = 50% Expected Conc. = 248 Median Pct Recovery = 50% Expected Conc. = 248 Median Pct Recovery = 50% Expected Conc. = 401 Median Pct Recovery = 50% Expected Conc. = 401 Median Pct Recovery = 50% Expected Conc. = 248 Median Pct Recovery = 50% Analysis Date = 03/15/17 SpikeMix = ERA 04121605: 0 µl & Abs 051816sed3H1: 0 µl Pct Recovery = 45% Analysis Date = 11/10/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 051816sed3H1: 0 µl Pct Recovery = 200% Analysis Date = 03/17/17 SpikeMix = Abs 050916sed3L3: 0 µl & ERA 04121604: 0 µl Pct Recovery = 54% Analysis Date = 03/17/17 SpikeMix = ERA 04121604: 0 µl & ERA 04121605: 0 µl Pct Recovery = 42% Analysis Date = 03/17/17 SpikeMix = ERA 04121606: 0 µl & ERA 04121604: 0 µl Pct Recovery = 40% Analysis Date = 02/21/17 SpikeMix = ERA 04121606: 0 µl & ERA 04121604: 0 µl Pct Recovery = 42% Analysis Date = 02/21/17 SpikeMix = ERA 04121604: 0 µl & Abs 050916sed3L2: 0 µl Pct Recovery = 54% Analysis Date = 02/10/17 SpikeMix = ERA 04121604: 0 µl & ERA 04121605: 0 µl Pct Recovery = 47% Analysis Date = 11/09/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 051816sed3L1: 0 µl Pct Recovery = 61% Analysis Date = 11/09/16 SpikeMix = Abs 051816sed3L1: 0 µl & Abs 050916sed3L2: 0 µl Pct Recovery = 61% Median Pct Recovery = 50% Median Pct Recovery = 50% Median Pct Recovery = 50% Median Pct Recovery = 50% Median Pct Recovery = 50% Median Pct Recovery = 50% Median Pct Recovery = 50% Median Pct Recovery = 50% Median Pct Recovery = 50% Median Pct Recovery = 50% Median Pct Recovery = 50% Median Pct Recovery = 50% Median Pct Recovery = 50% Median Pct Recovery = 50% Median Pct Recovery = 50% Median Pct Recovery = 50% Median Pct Recovery = 50% Median Pct Recovery = 50% Median Pct Recovery = 50% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
HEXAHYDROHEXAMETHYLCYCLOPENTABENZOPYRAN (HHCB)
METHOD: 5433 , TESTIDCODE: 63209GM008
DATES: 10/12/16 - 03/17/17
Open Data Set

Expected Conc. = 402 Median Pct Recovery = 32% Expected Conc. = 402 Median Pct Recovery = 32% Expected Conc. = 402 Median Pct Recovery = 32% Expected Conc. = 249 Median Pct Recovery = 32% Expected Conc. = 249 Median Pct Recovery = 32% Expected Conc. = 249 Median Pct Recovery = 32% Expected Conc. = 249 Median Pct Recovery = 32% Expected Conc. = 249 Median Pct Recovery = 32% Expected Conc. = 249 Median Pct Recovery = 32% Expected Conc. = 249 Median Pct Recovery = 32% Expected Conc. = 249 Median Pct Recovery = 32% Expected Conc. = 249 Median Pct Recovery = 32% Expected Conc. = 249 Median Pct Recovery = 32% Expected Conc. = 249 Median Pct Recovery = 32% Expected Conc. = 249 Median Pct Recovery = 32% Expected Conc. = 249 Median Pct Recovery = 32% Expected Conc. = 249 Median Pct Recovery = 32% Expected Conc. = 249 Median Pct Recovery = 32% Expected Conc. = 249 Median Pct Recovery = 32% Expected Conc. = 402 Median Pct Recovery = 32% Expected Conc. = 402 Median Pct Recovery = 32% Expected Conc. = 249 Median Pct Recovery = 32% Analysis Date = 11/09/16 SpikeMix = Abs 050916sed3H2: 0 µl & Abs 050916sed3L3: 0 µl Pct Recovery = 33% Analysis Date = 10/12/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 050916sed3H2: 0 µl Pct Recovery = 38% Analysis Date = 03/17/17 SpikeMix = ERA 04121604: 0 µl & ERA 04121605: 0 µl Pct Recovery = 29% Analysis Date = 03/17/17 SpikeMix = ERA 04121605: 0 µl Pct Recovery = 58% Analysis Date = 03/15/17 SpikeMix = ERA 04121605: 0 µl & ERA 04121606: 0 µl Pct Recovery = 28% Analysis Date = 03/15/17 SpikeMix = ERA 04121605: 0 µl & Abs 051816sed3H1: 0 µl Pct Recovery = 30% Analysis Date = 02/21/17 SpikeMix = ERA 04121604: 0 µl & Abs 050916sed3L2: 0 µl Pct Recovery = 34% Analysis Date = 02/10/17 SpikeMix = ERA 04121604: 0 µl & ERA 04121605: 0 µl Pct Recovery = 30% Analysis Date = 02/10/17 SpikeMix = ERA 04121605: 0 µl & ERA 04121606: 0 µl Pct Recovery = 31% Analysis Date = 11/09/16 SpikeMix = Abs 051816sed3L1: 0 µl & Abs 050916sed3L2: 0 µl Pct Recovery = 35% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
INDOLE
METHOD: 5433 , TESTIDCODE: 63210GM008
DATES: 11/09/16 - 03/17/17
Open Data Set

Expected Conc. = 802 Median Pct Recovery = 31% Expected Conc. = 802 Median Pct Recovery = 31% Expected Conc. = 802 Median Pct Recovery = 31% Expected Conc. = 505 Median Pct Recovery = 31% Expected Conc. = 505 Median Pct Recovery = 31% Expected Conc. = 505 Median Pct Recovery = 31% Expected Conc. = 505 Median Pct Recovery = 31% Expected Conc. = 499 Median Pct Recovery = 31% Expected Conc. = 499 Median Pct Recovery = 31% Expected Conc. = 499 Median Pct Recovery = 31% Expected Conc. = 499 Median Pct Recovery = 31% Expected Conc. = 499 Median Pct Recovery = 31% Expected Conc. = 499 Median Pct Recovery = 31% Expected Conc. = 499 Median Pct Recovery = 31% Expected Conc. = 499 Median Pct Recovery = 31% Expected Conc. = 499 Median Pct Recovery = 31% Expected Conc. = 499 Median Pct Recovery = 31% Expected Conc. = 499 Median Pct Recovery = 31% Expected Conc. = 499 Median Pct Recovery = 31% Expected Conc. = 802 Median Pct Recovery = 31% Expected Conc. = 802 Median Pct Recovery = 31% Expected Conc. = 505 Median Pct Recovery = 31% Analysis Date = 03/15/17 SpikeMix = ERA 04121605: 0 µl & Abs 051816sed3H1: 0 µl Pct Recovery = 30% Analysis Date = 11/10/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 051816sed3H1: 0 µl Pct Recovery = 22% Analysis Date = 11/09/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 051816sed3L1: 0 µl Pct Recovery = 27% Analysis Date = 11/09/16 SpikeMix = Abs 051816sed3L1: 0 µl & Abs 050916sed3L2: 0 µl Pct Recovery = 32% Analysis Date = 03/17/17 SpikeMix = Abs 050916sed3L3: 0 µl & ERA 04121604: 0 µl Pct Recovery = 47% Analysis Date = 03/17/17 SpikeMix = ERA 04121604: 0 µl & ERA 04121605: 0 µl Pct Recovery = 25% Analysis Date = 03/17/17 SpikeMix = ERA 04121606: 0 µl & ERA 04121604: 0 µl Pct Recovery = 28% Analysis Date = 02/21/17 SpikeMix = ERA 04121606: 0 µl & ERA 04121604: 0 µl Pct Recovery = 36% Analysis Date = 02/21/17 SpikeMix = ERA 04121604: 0 µl & Abs 050916sed3L2: 0 µl Pct Recovery = 50% Analysis Date = 02/10/17 SpikeMix = ERA 04121604: 0 µl & ERA 04121605: 0 µl Pct Recovery = 34% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
ISOBORNEOL
METHOD: 5433 , TESTIDCODE: 63211GM008
DATES: 10/12/16 - 03/17/17
Open Data Set

Expected Conc. = 401 Median Pct Recovery = 32% Expected Conc. = 401 Median Pct Recovery = 32% Expected Conc. = 401 Median Pct Recovery = 32% Expected Conc. = 250 Median Pct Recovery = 32% Expected Conc. = 250 Median Pct Recovery = 32% Expected Conc. = 250 Median Pct Recovery = 32% Expected Conc. = 250 Median Pct Recovery = 32% Expected Conc. = 250 Median Pct Recovery = 32% Expected Conc. = 250 Median Pct Recovery = 32% Expected Conc. = 250 Median Pct Recovery = 32% Expected Conc. = 250 Median Pct Recovery = 32% Expected Conc. = 250 Median Pct Recovery = 32% Expected Conc. = 250 Median Pct Recovery = 32% Expected Conc. = 250 Median Pct Recovery = 32% Expected Conc. = 250 Median Pct Recovery = 32% Expected Conc. = 249 Median Pct Recovery = 32% Expected Conc. = 249 Median Pct Recovery = 32% Expected Conc. = 249 Median Pct Recovery = 32% Expected Conc. = 249 Median Pct Recovery = 32% Expected Conc. = 401 Median Pct Recovery = 32% Expected Conc. = 401 Median Pct Recovery = 32% Expected Conc. = 249 Median Pct Recovery = 32% Analysis Date = 11/09/16 SpikeMix = Abs 050916sed3H2: 0 µl & Abs 050916sed3L3: 0 µl Pct Recovery = 24% Analysis Date = 10/12/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 050916sed3H2: 0 µl Pct Recovery = 34% Analysis Date = 03/17/17 SpikeMix = ERA 04121604: 0 µl & ERA 04121605: 0 µl Pct Recovery = 41% Analysis Date = 03/17/17 SpikeMix = ERA 04121605: 0 µl Pct Recovery = 88% Analysis Date = 03/15/17 SpikeMix = ERA 04121605: 0 µl & ERA 04121606: 0 µl Pct Recovery = 28% Analysis Date = 03/15/17 SpikeMix = ERA 04121605: 0 µl & Abs 051816sed3H1: 0 µl Pct Recovery = 23% Analysis Date = 02/10/17 SpikeMix = ERA 04121604: 0 µl & ERA 04121605: 0 µl Pct Recovery = 32% Analysis Date = 02/10/17 SpikeMix = ERA 04121605: 0 µl & ERA 04121606: 0 µl Pct Recovery = 33% Analysis Date = 02/21/17 SpikeMix = ERA 04121604: 0 µl & Abs 050916sed3L2: 0 µl Pct Recovery = 30% Analysis Date = 11/09/16 SpikeMix = Abs 051816sed3L1: 0 µl & Abs 050916sed3L2: 0 µl Pct Recovery = 40% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
ISOPHORONE
METHOD: 5433 , TESTIDCODE: 63212GM008
DATES: 10/12/16 - 03/17/17
Open Data Set

Expected Conc. = 400 Median Pct Recovery = 15% Expected Conc. = 400 Median Pct Recovery = 15% Expected Conc. = 400 Median Pct Recovery = 15% Expected Conc. = 400 Median Pct Recovery = 15% Expected Conc. = 400 Median Pct Recovery = 15% Expected Conc. = 250 Median Pct Recovery = 15% Expected Conc. = 250 Median Pct Recovery = 15% Expected Conc. = 250 Median Pct Recovery = 15% Expected Conc. = 250 Median Pct Recovery = 15% Expected Conc. = 250 Median Pct Recovery = 15% Expected Conc. = 250 Median Pct Recovery = 15% Expected Conc. = 250 Median Pct Recovery = 15% Expected Conc. = 250 Median Pct Recovery = 15% Expected Conc. = 250 Median Pct Recovery = 15% Expected Conc. = 250 Median Pct Recovery = 15% Expected Conc. = 248 Median Pct Recovery = 15% Expected Conc. = 248 Median Pct Recovery = 15% Expected Conc. = 248 Median Pct Recovery = 15% Expected Conc. = 248 Median Pct Recovery = 15% Expected Conc. = 250 Median Pct Recovery = 15% Expected Conc. = 250 Median Pct Recovery = 15% Expected Conc. = 248 Median Pct Recovery = 15% Analysis Date = 11/10/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 051816sed3H1: 0 µl Pct Recovery = 2% Analysis Date = 11/09/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 051816sed3L1: 0 µl Pct Recovery = 5% Analysis Date = 10/12/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 050916sed3H2: 0 µl Pct Recovery = 6% Analysis Date = 03/17/17 SpikeMix = ERA 04121606: 0 µl Pct Recovery = 70% Analysis Date = 03/17/17 SpikeMix = ERA 04121606: 0 µl & ERA 04121604: 0 µl Pct Recovery = 24% Analysis Date = 03/15/17 SpikeMix = ERA 04121605: 0 µl & ERA 04121606: 0 µl Pct Recovery = 35% Analysis Date = 02/21/17 SpikeMix = ERA 04121606: 0 µl & ERA 04121604: 0 µl Pct Recovery = 36% Analysis Date = 02/10/17 SpikeMix = ERA 04121605: 0 µl & ERA 04121606: 0 µl Pct Recovery = 31% Analysis Date = 03/17/17 SpikeMix = Abs 050916sed3L3: 0 µl & ERA 04121604: 0 µl Pct Recovery = 6% Analysis Date = 11/09/16 SpikeMix = Abs 050916sed3H2: 0 µl & Abs 050916sed3L3: 0 µl Pct Recovery = 5% Median Pct Recovery = 15% Median Pct Recovery = 15% Median Pct Recovery = 15% Median Pct Recovery = 15% Median Pct Recovery = 15% Median Pct Recovery = 15% Median Pct Recovery = 15% Median Pct Recovery = 15% Median Pct Recovery = 15% Median Pct Recovery = 15% Median Pct Recovery = 15% Median Pct Recovery = 15% Median Pct Recovery = 15% Median Pct Recovery = 15% Median Pct Recovery = 15% Median Pct Recovery = 15% Median Pct Recovery = 15% Median Pct Recovery = 15% Median Pct Recovery = 15% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
ISOPROPYLBENZENE (CUMENE)
METHOD: 5433 , TESTIDCODE: 63213GM008
DATES: 10/12/16 - 03/17/17
Open Data Set

Expected Conc. = 805 Median Pct Recovery = 7% Expected Conc. = 805 Median Pct Recovery = 7% Expected Conc. = 805 Median Pct Recovery = 7% Expected Conc. = 507 Median Pct Recovery = 7% Expected Conc. = 507 Median Pct Recovery = 7% Expected Conc. = 501 Median Pct Recovery = 7% Expected Conc. = 501 Median Pct Recovery = 7% Expected Conc. = 501 Median Pct Recovery = 7% Expected Conc. = 501 Median Pct Recovery = 7% Expected Conc. = 501 Median Pct Recovery = 7% Expected Conc. = 501 Median Pct Recovery = 7% Expected Conc. = 501 Median Pct Recovery = 7% Expected Conc. = 501 Median Pct Recovery = 7% Expected Conc. = 501 Median Pct Recovery = 7% Expected Conc. = 501 Median Pct Recovery = 7% Expected Conc. = 805 Median Pct Recovery = 7% Expected Conc. = 805 Median Pct Recovery = 7% Expected Conc. = 507 Median Pct Recovery = 7% Expected Conc. = 507 Median Pct Recovery = 7% Expected Conc. = 507 Median Pct Recovery = 7% Expected Conc. = 507 Median Pct Recovery = 7% Expected Conc. = 501 Median Pct Recovery = 7% Analysis Date = 11/09/16 SpikeMix = Abs 050916sed3H2: 0 µl & Abs 050916sed3L3: 0 µl Pct Recovery = 1% Analysis Date = 10/12/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 050916sed3H2: 0 µl Pct Recovery = 5% Analysis Date = 11/09/16 SpikeMix = Abs 051816sed3L1: 0 µl & Abs 050916sed3L2: 0 µl Pct Recovery = 3% Analysis Date = 03/17/17 SpikeMix = ERA 04121604: 0 µl & ERA 04121605: 0 µl Pct Recovery = 12% Analysis Date = 03/17/17 SpikeMix = ERA 04121605: 0 µl Pct Recovery = 20% Analysis Date = 03/15/17 SpikeMix = ERA 04121605: 0 µl & ERA 04121606: 0 µl Pct Recovery = 6% Analysis Date = 02/10/17 SpikeMix = ERA 04121604: 0 µl & ERA 04121605: 0 µl Pct Recovery = 9% Analysis Date = 02/10/17 SpikeMix = ERA 04121605: 0 µl & ERA 04121606: 0 µl Pct Recovery = 9% Median Pct Recovery = 7% Median Pct Recovery = 7% Median Pct Recovery = 7% Median Pct Recovery = 7% Median Pct Recovery = 7% Median Pct Recovery = 7% Median Pct Recovery = 7% Median Pct Recovery = 7% Median Pct Recovery = 7% Median Pct Recovery = 7% Median Pct Recovery = 7% Median Pct Recovery = 7% Median Pct Recovery = 7% Median Pct Recovery = 7% Median Pct Recovery = 7% Median Pct Recovery = 7% Median Pct Recovery = 7% Median Pct Recovery = 7% Median Pct Recovery = 7% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
ISOQUINOLINE
METHOD: 5433 , TESTIDCODE: 63214GM008
DATES: 10/12/16 - 03/17/17
Open Data Set

Expected Conc. = 803 Median Pct Recovery = 34% Expected Conc. = 803 Median Pct Recovery = 34% Expected Conc. = 803 Median Pct Recovery = 34% Expected Conc. = 506 Median Pct Recovery = 34% Expected Conc. = 506 Median Pct Recovery = 34% Expected Conc. = 506 Median Pct Recovery = 34% Expected Conc. = 506 Median Pct Recovery = 34% Expected Conc. = 498 Median Pct Recovery = 34% Expected Conc. = 498 Median Pct Recovery = 34% Expected Conc. = 498 Median Pct Recovery = 34% Expected Conc. = 498 Median Pct Recovery = 34% Expected Conc. = 498 Median Pct Recovery = 34% Expected Conc. = 498 Median Pct Recovery = 34% Expected Conc. = 498 Median Pct Recovery = 34% Expected Conc. = 498 Median Pct Recovery = 34% Expected Conc. = 498 Median Pct Recovery = 34% Expected Conc. = 498 Median Pct Recovery = 34% Expected Conc. = 498 Median Pct Recovery = 34% Expected Conc. = 498 Median Pct Recovery = 34% Expected Conc. = 803 Median Pct Recovery = 34% Expected Conc. = 803 Median Pct Recovery = 34% Expected Conc. = 506 Median Pct Recovery = 34% Analysis Date = 11/09/16 SpikeMix = Abs 050916sed3H2: 0 µl & Abs 050916sed3L3: 0 µl Pct Recovery = 9% Analysis Date = 10/12/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 050916sed3H2: 0 µl Pct Recovery = 13% Analysis Date = 02/21/17 SpikeMix = ERA 04121604: 0 µl & Abs 050916sed3L2: 0 µl Pct Recovery = 38% Analysis Date = 11/09/16 SpikeMix = Abs 051816sed3L1: 0 µl & Abs 050916sed3L2: 0 µl Pct Recovery = 5% Analysis Date = 03/17/17 SpikeMix = ERA 04121604: 0 µl & ERA 04121605: 0 µl Pct Recovery = 29% Analysis Date = 03/17/17 SpikeMix = ERA 04121605: 0 µl Pct Recovery = 66% Analysis Date = 03/15/17 SpikeMix = ERA 04121605: 0 µl & ERA 04121606: 0 µl Pct Recovery = 35% Analysis Date = 03/15/17 SpikeMix = ERA 04121605: 0 µl & Abs 051816sed3H1: 0 µl Pct Recovery = 33% Analysis Date = 02/10/17 SpikeMix = ERA 04121604: 0 µl & ERA 04121605: 0 µl Pct Recovery = 39% Analysis Date = 02/10/17 SpikeMix = ERA 04121605: 0 µl & ERA 04121606: 0 µl Pct Recovery = 40% Median Pct Recovery = 34% Median Pct Recovery = 34% Median Pct Recovery = 34% Median Pct Recovery = 34% Median Pct Recovery = 34% Median Pct Recovery = 34% Median Pct Recovery = 34% Median Pct Recovery = 34% Median Pct Recovery = 34% Median Pct Recovery = 34% Median Pct Recovery = 34% Median Pct Recovery = 34% Median Pct Recovery = 34% Median Pct Recovery = 34% Median Pct Recovery = 34% Median Pct Recovery = 34% Median Pct Recovery = 34% Median Pct Recovery = 34% Median Pct Recovery = 34% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
MENTHOL
METHOD: 5433 , TESTIDCODE: 63215GM008
DATES: 10/12/16 - 03/17/17
Open Data Set

Expected Conc. = 402 Median Pct Recovery = 32% Expected Conc. = 402 Median Pct Recovery = 32% Expected Conc. = 402 Median Pct Recovery = 32% Expected Conc. = 402 Median Pct Recovery = 32% Expected Conc. = 402 Median Pct Recovery = 32% Expected Conc. = 251 Median Pct Recovery = 32% Expected Conc. = 251 Median Pct Recovery = 32% Expected Conc. = 251 Median Pct Recovery = 32% Expected Conc. = 251 Median Pct Recovery = 32% Expected Conc. = 251 Median Pct Recovery = 32% Expected Conc. = 251 Median Pct Recovery = 32% Expected Conc. = 251 Median Pct Recovery = 32% Expected Conc. = 251 Median Pct Recovery = 32% Expected Conc. = 249 Median Pct Recovery = 32% Expected Conc. = 249 Median Pct Recovery = 32% Expected Conc. = 249 Median Pct Recovery = 32% Expected Conc. = 249 Median Pct Recovery = 32% Expected Conc. = 251 Median Pct Recovery = 32% Expected Conc. = 251 Median Pct Recovery = 32% Expected Conc. = 251 Median Pct Recovery = 32% Expected Conc. = 251 Median Pct Recovery = 32% Expected Conc. = 249 Median Pct Recovery = 32% Analysis Date = 11/10/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 051816sed3H1: 0 µl Pct Recovery = 11% Analysis Date = 11/09/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 051816sed3L1: 0 µl Pct Recovery = 35% Analysis Date = 10/12/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 050916sed3H2: 0 µl Pct Recovery = 30% Analysis Date = 03/17/17 SpikeMix = ERA 04121606: 0 µl Pct Recovery = 92% Analysis Date = 03/17/17 SpikeMix = ERA 04121606: 0 µl & ERA 04121604: 0 µl Pct Recovery = 38% Analysis Date = 02/21/17 SpikeMix = ERA 04121606: 0 µl & ERA 04121604: 0 µl Pct Recovery = 35% Analysis Date = 02/10/17 SpikeMix = ERA 04121605: 0 µl & ERA 04121606: 0 µl Pct Recovery = 16% Analysis Date = 03/17/17 SpikeMix = Abs 050916sed3L3: 0 µl & ERA 04121604: 0 µl Pct Recovery = 32% Analysis Date = 11/09/16 SpikeMix = Abs 050916sed3H2: 0 µl & Abs 050916sed3L3: 0 µl Pct Recovery = 30% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
METOLACHLOR
METHOD: 5433 , TESTIDCODE: 63218GM008
DATES: 10/12/16 - 03/17/17
Open Data Set

Expected Conc. = 400 Median Pct Recovery = 39% Expected Conc. = 400 Median Pct Recovery = 39% Expected Conc. = 400 Median Pct Recovery = 39% Expected Conc. = 400 Median Pct Recovery = 39% Expected Conc. = 400 Median Pct Recovery = 39% Expected Conc. = 253 Median Pct Recovery = 39% Expected Conc. = 253 Median Pct Recovery = 39% Expected Conc. = 253 Median Pct Recovery = 39% Expected Conc. = 253 Median Pct Recovery = 39% Expected Conc. = 253 Median Pct Recovery = 39% Expected Conc. = 253 Median Pct Recovery = 39% Expected Conc. = 253 Median Pct Recovery = 39% Expected Conc. = 253 Median Pct Recovery = 39% Expected Conc. = 253 Median Pct Recovery = 39% Expected Conc. = 253 Median Pct Recovery = 39% Expected Conc. = 248 Median Pct Recovery = 39% Expected Conc. = 248 Median Pct Recovery = 39% Expected Conc. = 248 Median Pct Recovery = 39% Expected Conc. = 248 Median Pct Recovery = 39% Expected Conc. = 253 Median Pct Recovery = 39% Expected Conc. = 253 Median Pct Recovery = 39% Expected Conc. = 248 Median Pct Recovery = 39% Analysis Date = 11/10/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 051816sed3H1: 0 µl Pct Recovery = 18% Analysis Date = 11/09/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 051816sed3L1: 0 µl Pct Recovery = 40% Analysis Date = 10/12/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 050916sed3H2: 0 µl Pct Recovery = 42% Analysis Date = 03/17/17 SpikeMix = ERA 04121606: 0 µl Pct Recovery = 77% Analysis Date = 03/17/17 SpikeMix = ERA 04121606: 0 µl & ERA 04121604: 0 µl Pct Recovery = 38% Analysis Date = 03/15/17 SpikeMix = ERA 04121605: 0 µl & ERA 04121606: 0 µl Pct Recovery = 38% Analysis Date = 02/21/17 SpikeMix = ERA 04121606: 0 µl & ERA 04121604: 0 µl Pct Recovery = 41% Analysis Date = 02/10/17 SpikeMix = ERA 04121605: 0 µl & ERA 04121606: 0 µl Pct Recovery = 43% Analysis Date = 03/17/17 SpikeMix = Abs 050916sed3L3: 0 µl & ERA 04121604: 0 µl Pct Recovery = 38% Analysis Date = 11/09/16 SpikeMix = Abs 050916sed3H2: 0 µl & Abs 050916sed3L3: 0 µl Pct Recovery = 39% Median Pct Recovery = 39% Median Pct Recovery = 39% Median Pct Recovery = 39% Median Pct Recovery = 39% Median Pct Recovery = 39% Median Pct Recovery = 39% Median Pct Recovery = 39% Median Pct Recovery = 39% Median Pct Recovery = 39% Median Pct Recovery = 39% Median Pct Recovery = 39% Median Pct Recovery = 39% Median Pct Recovery = 39% Median Pct Recovery = 39% Median Pct Recovery = 39% Median Pct Recovery = 39% Median Pct Recovery = 39% Median Pct Recovery = 39% Median Pct Recovery = 39% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
N,N-DIETHYL-META-TOLUAMIDE (DEET)
METHOD: 5433 , TESTIDCODE: 63219GM008
DATES: 11/09/16 - 03/17/17
Open Data Set

Expected Conc. = 801 Median Pct Recovery = 40% Expected Conc. = 801 Median Pct Recovery = 40% Expected Conc. = 801 Median Pct Recovery = 40% Expected Conc. = 505 Median Pct Recovery = 40% Expected Conc. = 505 Median Pct Recovery = 40% Expected Conc. = 505 Median Pct Recovery = 40% Expected Conc. = 505 Median Pct Recovery = 40% Expected Conc. = 501 Median Pct Recovery = 40% Expected Conc. = 501 Median Pct Recovery = 40% Expected Conc. = 501 Median Pct Recovery = 40% Expected Conc. = 501 Median Pct Recovery = 40% Expected Conc. = 501 Median Pct Recovery = 40% Expected Conc. = 501 Median Pct Recovery = 40% Expected Conc. = 501 Median Pct Recovery = 40% Expected Conc. = 501 Median Pct Recovery = 40% Expected Conc. = 501 Median Pct Recovery = 40% Expected Conc. = 501 Median Pct Recovery = 40% Expected Conc. = 501 Median Pct Recovery = 40% Expected Conc. = 501 Median Pct Recovery = 40% Expected Conc. = 801 Median Pct Recovery = 40% Expected Conc. = 801 Median Pct Recovery = 40% Expected Conc. = 505 Median Pct Recovery = 40% Analysis Date = 03/15/17 SpikeMix = ERA 04121605: 0 µl & Abs 051816sed3H1: 0 µl Pct Recovery = 37% Analysis Date = 11/10/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 051816sed3H1: 0 µl Pct Recovery = 14% Analysis Date = 11/09/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 051816sed3L1: 0 µl Pct Recovery = 12% Analysis Date = 11/09/16 SpikeMix = Abs 051816sed3L1: 0 µl & Abs 050916sed3L2: 0 µl Pct Recovery = 14% Analysis Date = 03/17/17 SpikeMix = Abs 050916sed3L3: 0 µl & ERA 04121604: 0 µl Pct Recovery = 14% Analysis Date = 03/17/17 SpikeMix = ERA 04121604: 0 µl & ERA 04121605: 0 µl Pct Recovery = 45% Analysis Date = 03/17/17 SpikeMix = ERA 04121606: 0 µl & ERA 04121604: 0 µl Pct Recovery = 43% Analysis Date = 02/21/17 SpikeMix = ERA 04121606: 0 µl & ERA 04121604: 0 µl Pct Recovery = 45% Analysis Date = 02/21/17 SpikeMix = ERA 04121604: 0 µl & Abs 050916sed3L2: 0 µl Pct Recovery = 46% Analysis Date = 02/10/17 SpikeMix = ERA 04121604: 0 µl & ERA 04121605: 0 µl Pct Recovery = 50% Median Pct Recovery = 40% Median Pct Recovery = 40% Median Pct Recovery = 40% Median Pct Recovery = 40% Median Pct Recovery = 40% Median Pct Recovery = 40% Median Pct Recovery = 40% Median Pct Recovery = 40% Median Pct Recovery = 40% Median Pct Recovery = 40% Median Pct Recovery = 40% Median Pct Recovery = 40% Median Pct Recovery = 40% Median Pct Recovery = 40% Median Pct Recovery = 40% Median Pct Recovery = 40% Median Pct Recovery = 40% Median Pct Recovery = 40% Median Pct Recovery = 40% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
NAPHTHALENE
METHOD: 5433 , TESTIDCODE: 63220GM008
DATES: 11/09/16 - 03/17/17
Open Data Set

Expected Conc. = 400 Median Pct Recovery = 30% Expected Conc. = 400 Median Pct Recovery = 30% Expected Conc. = 400 Median Pct Recovery = 30% Expected Conc. = 249 Median Pct Recovery = 30% Expected Conc. = 249 Median Pct Recovery = 30% Expected Conc. = 249 Median Pct Recovery = 30% Expected Conc. = 249 Median Pct Recovery = 30% Expected Conc. = 249 Median Pct Recovery = 30% Expected Conc. = 249 Median Pct Recovery = 30% Expected Conc. = 249 Median Pct Recovery = 30% Expected Conc. = 249 Median Pct Recovery = 30% Expected Conc. = 249 Median Pct Recovery = 30% Expected Conc. = 249 Median Pct Recovery = 30% Expected Conc. = 249 Median Pct Recovery = 30% Expected Conc. = 249 Median Pct Recovery = 30% Expected Conc. = 248 Median Pct Recovery = 30% Expected Conc. = 248 Median Pct Recovery = 30% Expected Conc. = 248 Median Pct Recovery = 30% Expected Conc. = 248 Median Pct Recovery = 30% Expected Conc. = 400 Median Pct Recovery = 30% Expected Conc. = 400 Median Pct Recovery = 30% Expected Conc. = 248 Median Pct Recovery = 30% Analysis Date = 03/15/17 SpikeMix = ERA 04121605: 0 µl & Abs 051816sed3H1: 0 µl Pct Recovery = 22% Analysis Date = 11/10/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 051816sed3H1: 0 µl Pct Recovery = 10% Analysis Date = 03/17/17 SpikeMix = Abs 050916sed3L3: 0 µl & ERA 04121604: 0 µl Pct Recovery = 33% Analysis Date = 03/17/17 SpikeMix = ERA 04121604: 0 µl & ERA 04121605: 0 µl Pct Recovery = 34% Analysis Date = 03/17/17 SpikeMix = ERA 04121606: 0 µl & ERA 04121604: 0 µl Pct Recovery = 30% Analysis Date = 02/21/17 SpikeMix = ERA 04121606: 0 µl & ERA 04121604: 0 µl Pct Recovery = 28% Analysis Date = 02/21/17 SpikeMix = ERA 04121604: 0 µl & Abs 050916sed3L2: 0 µl Pct Recovery = 27% Analysis Date = 02/10/17 SpikeMix = ERA 04121604: 0 µl & ERA 04121605: 0 µl Pct Recovery = 32% Analysis Date = 11/09/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 051816sed3L1: 0 µl Pct Recovery = 30% Analysis Date = 11/09/16 SpikeMix = Abs 051816sed3L1: 0 µl & Abs 050916sed3L2: 0 µl Pct Recovery = 32% Median Pct Recovery = 30% Median Pct Recovery = 30% Median Pct Recovery = 30% Median Pct Recovery = 30% Median Pct Recovery = 30% Median Pct Recovery = 30% Median Pct Recovery = 30% Median Pct Recovery = 30% Median Pct Recovery = 30% Median Pct Recovery = 30% Median Pct Recovery = 30% Median Pct Recovery = 30% Median Pct Recovery = 30% Median Pct Recovery = 30% Median Pct Recovery = 30% Median Pct Recovery = 30% Median Pct Recovery = 30% Median Pct Recovery = 30% Median Pct Recovery = 30% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
P-CRESOL
METHOD: 5433 , TESTIDCODE: 63222GM008
DATES: 10/12/16 - 03/17/17
Open Data Set

Expected Conc. = 2012 Median Pct Recovery = 43% Expected Conc. = 2012 Median Pct Recovery = 43% Expected Conc. = 2012 Median Pct Recovery = 43% Expected Conc. = 2012 Median Pct Recovery = 43% Expected Conc. = 2012 Median Pct Recovery = 43% Expected Conc. = 1259 Median Pct Recovery = 43% Expected Conc. = 1259 Median Pct Recovery = 43% Expected Conc. = 1259 Median Pct Recovery = 43% Expected Conc. = 1259 Median Pct Recovery = 43% Expected Conc. = 1250 Median Pct Recovery = 43% Expected Conc. = 1250 Median Pct Recovery = 43% Expected Conc. = 1250 Median Pct Recovery = 43% Expected Conc. = 1250 Median Pct Recovery = 43% Expected Conc. = 1250 Median Pct Recovery = 43% Expected Conc. = 1250 Median Pct Recovery = 43% Expected Conc. = 1250 Median Pct Recovery = 43% Expected Conc. = 1250 Median Pct Recovery = 43% Expected Conc. = 1250 Median Pct Recovery = 43% Expected Conc. = 1250 Median Pct Recovery = 43% Expected Conc. = 1259 Median Pct Recovery = 43% Expected Conc. = 1259 Median Pct Recovery = 43% Expected Conc. = 1250 Median Pct Recovery = 43% Analysis Date = 11/10/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 051816sed3H1: 0 µl Pct Recovery = 31% Analysis Date = 11/09/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 051816sed3L1: 0 µl Pct Recovery = 47% Analysis Date = 10/12/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 050916sed3H2: 0 µl Pct Recovery = 51% Analysis Date = 03/17/17 SpikeMix = Abs 050916sed3L3: 0 µl & ERA 04121604: 0 µl Pct Recovery = 44% Analysis Date = 11/09/16 SpikeMix = Abs 050916sed3H2: 0 µl & Abs 050916sed3L3: 0 µl Pct Recovery = 51% Analysis Date = 03/17/17 SpikeMix = ERA 04121606: 0 µl Pct Recovery = 72% Analysis Date = 03/17/17 SpikeMix = ERA 04121606: 0 µl & ERA 04121604: 0 µl Pct Recovery = 35% Analysis Date = 03/15/17 SpikeMix = ERA 04121605: 0 µl & ERA 04121606: 0 µl Pct Recovery = 40% Analysis Date = 02/21/17 SpikeMix = ERA 04121606: 0 µl & ERA 04121604: 0 µl Pct Recovery = 39% Analysis Date = 02/10/17 SpikeMix = ERA 04121605: 0 µl & ERA 04121606: 0 µl Pct Recovery = 42% Median Pct Recovery = 43% Median Pct Recovery = 43% Median Pct Recovery = 43% Median Pct Recovery = 43% Median Pct Recovery = 43% Median Pct Recovery = 43% Median Pct Recovery = 43% Median Pct Recovery = 43% Median Pct Recovery = 43% Median Pct Recovery = 43% Median Pct Recovery = 43% Median Pct Recovery = 43% Median Pct Recovery = 43% Median Pct Recovery = 43% Median Pct Recovery = 43% Median Pct Recovery = 43% Median Pct Recovery = 43% Median Pct Recovery = 43% Median Pct Recovery = 43% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
PHENANTHRENE
METHOD: 5433 , TESTIDCODE: 63224GM008
DATES: 10/12/16 - 03/17/17
Open Data Set

Expected Conc. = 401 Median Pct Recovery = 42% Expected Conc. = 401 Median Pct Recovery = 42% Expected Conc. = 401 Median Pct Recovery = 42% Expected Conc. = 250 Median Pct Recovery = 42% Expected Conc. = 250 Median Pct Recovery = 42% Expected Conc. = 250 Median Pct Recovery = 42% Expected Conc. = 250 Median Pct Recovery = 42% Expected Conc. = 250 Median Pct Recovery = 42% Expected Conc. = 250 Median Pct Recovery = 42% Expected Conc. = 250 Median Pct Recovery = 42% Expected Conc. = 250 Median Pct Recovery = 42% Expected Conc. = 250 Median Pct Recovery = 42% Expected Conc. = 250 Median Pct Recovery = 42% Expected Conc. = 250 Median Pct Recovery = 42% Expected Conc. = 250 Median Pct Recovery = 42% Expected Conc. = 249 Median Pct Recovery = 42% Expected Conc. = 249 Median Pct Recovery = 42% Expected Conc. = 249 Median Pct Recovery = 42% Expected Conc. = 249 Median Pct Recovery = 42% Expected Conc. = 401 Median Pct Recovery = 42% Expected Conc. = 401 Median Pct Recovery = 42% Expected Conc. = 249 Median Pct Recovery = 42% Analysis Date = 11/09/16 SpikeMix = Abs 050916sed3H2: 0 µl & Abs 050916sed3L3: 0 µl Pct Recovery = 43% Analysis Date = 10/12/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 050916sed3H2: 0 µl Pct Recovery = 51% Analysis Date = 03/17/17 SpikeMix = ERA 04121604: 0 µl & ERA 04121605: 0 µl Pct Recovery = 38% Analysis Date = 03/17/17 SpikeMix = ERA 04121605: 0 µl Pct Recovery = 74% Analysis Date = 03/15/17 SpikeMix = ERA 04121605: 0 µl & ERA 04121606: 0 µl Pct Recovery = 36% Analysis Date = 03/15/17 SpikeMix = ERA 04121605: 0 µl & Abs 051816sed3H1: 0 µl Pct Recovery = 41% Analysis Date = 02/10/17 SpikeMix = ERA 04121604: 0 µl & ERA 04121605: 0 µl Pct Recovery = 41% Analysis Date = 02/10/17 SpikeMix = ERA 04121605: 0 µl & ERA 04121606: 0 µl Pct Recovery = 43% Analysis Date = 02/21/17 SpikeMix = ERA 04121604: 0 µl & Abs 050916sed3L2: 0 µl Pct Recovery = 41% Analysis Date = 11/09/16 SpikeMix = Abs 051816sed3L1: 0 µl & Abs 050916sed3L2: 0 µl Pct Recovery = 53% Median Pct Recovery = 42% Median Pct Recovery = 42% Median Pct Recovery = 42% Median Pct Recovery = 42% Median Pct Recovery = 42% Median Pct Recovery = 42% Median Pct Recovery = 42% Median Pct Recovery = 42% Median Pct Recovery = 42% Median Pct Recovery = 42% Median Pct Recovery = 42% Median Pct Recovery = 42% Median Pct Recovery = 42% Median Pct Recovery = 42% Median Pct Recovery = 42% Median Pct Recovery = 42% Median Pct Recovery = 42% Median Pct Recovery = 42% Median Pct Recovery = 42% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
PROMETON
METHOD: 5433 , TESTIDCODE: 63226GM008
DATES: 10/12/16 - 03/17/17
Open Data Set

Expected Conc. = 401 Median Pct Recovery = 41% Expected Conc. = 401 Median Pct Recovery = 41% Expected Conc. = 401 Median Pct Recovery = 41% Expected Conc. = 249 Median Pct Recovery = 41% Expected Conc. = 249 Median Pct Recovery = 41% Expected Conc. = 249 Median Pct Recovery = 41% Expected Conc. = 249 Median Pct Recovery = 41% Expected Conc. = 249 Median Pct Recovery = 41% Expected Conc. = 249 Median Pct Recovery = 41% Expected Conc. = 249 Median Pct Recovery = 41% Expected Conc. = 249 Median Pct Recovery = 41% Expected Conc. = 249 Median Pct Recovery = 41% Expected Conc. = 249 Median Pct Recovery = 41% Expected Conc. = 249 Median Pct Recovery = 41% Expected Conc. = 249 Median Pct Recovery = 41% Expected Conc. = 249 Median Pct Recovery = 41% Expected Conc. = 249 Median Pct Recovery = 41% Expected Conc. = 401 Median Pct Recovery = 41% Expected Conc. = 401 Median Pct Recovery = 41% Expected Conc. = 249 Median Pct Recovery = 41% Expected Conc. = 249 Median Pct Recovery = 41% Expected Conc. = 249 Median Pct Recovery = 41% Analysis Date = 11/09/16 SpikeMix = Abs 050916sed3H2: 0 µl & Abs 050916sed3L3: 0 µl Pct Recovery = 15% Analysis Date = 10/12/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 050916sed3H2: 0 µl Pct Recovery = 37% Analysis Date = 03/17/17 SpikeMix = ERA 04121604: 0 µl & ERA 04121605: 0 µl Pct Recovery = 44% Analysis Date = 03/17/17 SpikeMix = ERA 04121605: 0 µl Pct Recovery = 81% Analysis Date = 03/15/17 SpikeMix = ERA 04121605: 0 µl & ERA 04121606: 0 µl Pct Recovery = 37% Analysis Date = 03/15/17 SpikeMix = ERA 04121605: 0 µl & Abs 051816sed3H1: 0 µl Pct Recovery = 36% Analysis Date = 02/21/17 SpikeMix = ERA 04121604: 0 µl & Abs 050916sed3L2: 0 µl Pct Recovery = 46% Analysis Date = 02/10/17 SpikeMix = ERA 04121604: 0 µl & ERA 04121605: 0 µl Pct Recovery = 45% Analysis Date = 02/10/17 SpikeMix = ERA 04121605: 0 µl & ERA 04121606: 0 µl Pct Recovery = 41% Median Pct Recovery = 41% Median Pct Recovery = 41% Median Pct Recovery = 41% Median Pct Recovery = 41% Median Pct Recovery = 41% Median Pct Recovery = 41% Median Pct Recovery = 41% Median Pct Recovery = 41% Median Pct Recovery = 41% Median Pct Recovery = 41% Median Pct Recovery = 41% Median Pct Recovery = 41% Median Pct Recovery = 41% Median Pct Recovery = 41% Median Pct Recovery = 41% Median Pct Recovery = 41% Median Pct Recovery = 41% Median Pct Recovery = 41% Median Pct Recovery = 41% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
PYRENE
METHOD: 5433 , TESTIDCODE: 63227GM008
DATES: 10/12/16 - 03/17/17
Open Data Set

Expected Conc. = 401 Median Pct Recovery = 44% Expected Conc. = 401 Median Pct Recovery = 44% Expected Conc. = 401 Median Pct Recovery = 44% Expected Conc. = 252 Median Pct Recovery = 44% Expected Conc. = 252 Median Pct Recovery = 44% Expected Conc. = 252 Median Pct Recovery = 44% Expected Conc. = 252 Median Pct Recovery = 44% Expected Conc. = 252 Median Pct Recovery = 44% Expected Conc. = 252 Median Pct Recovery = 44% Expected Conc. = 252 Median Pct Recovery = 44% Expected Conc. = 252 Median Pct Recovery = 44% Expected Conc. = 252 Median Pct Recovery = 44% Expected Conc. = 252 Median Pct Recovery = 44% Expected Conc. = 252 Median Pct Recovery = 44% Expected Conc. = 252 Median Pct Recovery = 44% Expected Conc. = 249 Median Pct Recovery = 44% Expected Conc. = 249 Median Pct Recovery = 44% Expected Conc. = 249 Median Pct Recovery = 44% Expected Conc. = 249 Median Pct Recovery = 44% Expected Conc. = 401 Median Pct Recovery = 44% Expected Conc. = 401 Median Pct Recovery = 44% Expected Conc. = 249 Median Pct Recovery = 44% Analysis Date = 11/09/16 SpikeMix = Abs 050916sed3H2: 0 µl & Abs 050916sed3L3: 0 µl Pct Recovery = 44% Analysis Date = 10/12/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 050916sed3H2: 0 µl Pct Recovery = 52% Analysis Date = 03/17/17 SpikeMix = ERA 04121604: 0 µl & ERA 04121605: 0 µl Pct Recovery = 38% Analysis Date = 03/17/17 SpikeMix = ERA 04121605: 0 µl Pct Recovery = 69% Analysis Date = 03/15/17 SpikeMix = ERA 04121605: 0 µl & ERA 04121606: 0 µl Pct Recovery = 35% Analysis Date = 03/15/17 SpikeMix = ERA 04121605: 0 µl & Abs 051816sed3H1: 0 µl Pct Recovery = 43% Analysis Date = 02/10/17 SpikeMix = ERA 04121604: 0 µl & ERA 04121605: 0 µl Pct Recovery = 40% Analysis Date = 02/10/17 SpikeMix = ERA 04121605: 0 µl & ERA 04121606: 0 µl Pct Recovery = 40% Analysis Date = 02/21/17 SpikeMix = ERA 04121604: 0 µl & Abs 050916sed3L2: 0 µl Pct Recovery = 46% Analysis Date = 11/09/16 SpikeMix = Abs 051816sed3L1: 0 µl & Abs 050916sed3L2: 0 µl Pct Recovery = 52% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
TRIS(2-BUTOXYETHYL)PHOSPHATE
METHOD: 5433 , TESTIDCODE: 63229GM008
DATES: 10/12/16 - 03/17/17
Open Data Set

Expected Conc. = 1211 Median Pct Recovery = 27% Expected Conc. = 1211 Median Pct Recovery = 27% Expected Conc. = 1211 Median Pct Recovery = 27% Expected Conc. = 1211 Median Pct Recovery = 27% Expected Conc. = 1211 Median Pct Recovery = 27% Expected Conc. = 752 Median Pct Recovery = 27% Expected Conc. = 752 Median Pct Recovery = 27% Expected Conc. = 752 Median Pct Recovery = 27% Expected Conc. = 752 Median Pct Recovery = 27% Expected Conc. = 750 Median Pct Recovery = 27% Expected Conc. = 750 Median Pct Recovery = 27% Expected Conc. = 750 Median Pct Recovery = 27% Expected Conc. = 750 Median Pct Recovery = 27% Expected Conc. = 750 Median Pct Recovery = 27% Expected Conc. = 750 Median Pct Recovery = 27% Expected Conc. = 750 Median Pct Recovery = 27% Expected Conc. = 750 Median Pct Recovery = 27% Expected Conc. = 750 Median Pct Recovery = 27% Expected Conc. = 750 Median Pct Recovery = 27% Expected Conc. = 752 Median Pct Recovery = 27% Expected Conc. = 752 Median Pct Recovery = 27% Expected Conc. = 750 Median Pct Recovery = 27% Analysis Date = 11/10/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 051816sed3H1: 0 µl Pct Recovery = 10% Analysis Date = 11/09/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 051816sed3L1: 0 µl Pct Recovery = 20% Analysis Date = 10/12/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 050916sed3H2: 0 µl Pct Recovery = 53% Analysis Date = 03/17/17 SpikeMix = Abs 050916sed3L3: 0 µl & ERA 04121604: 0 µl Pct Recovery = 28% Analysis Date = 11/09/16 SpikeMix = Abs 050916sed3H2: 0 µl & Abs 050916sed3L3: 0 µl Pct Recovery = 23% Analysis Date = 03/17/17 SpikeMix = ERA 04121606: 0 µl Pct Recovery = 67% Analysis Date = 03/17/17 SpikeMix = ERA 04121606: 0 µl & ERA 04121604: 0 µl Pct Recovery = 27% Analysis Date = 03/15/17 SpikeMix = ERA 04121605: 0 µl & ERA 04121606: 0 µl Pct Recovery = 29% Analysis Date = 02/21/17 SpikeMix = ERA 04121606: 0 µl & ERA 04121604: 0 µl Pct Recovery = 35% Analysis Date = 02/10/17 SpikeMix = ERA 04121605: 0 µl & ERA 04121606: 0 µl Pct Recovery = 25% Median Pct Recovery = 27% Median Pct Recovery = 27% Median Pct Recovery = 27% Median Pct Recovery = 27% Median Pct Recovery = 27% Median Pct Recovery = 27% Median Pct Recovery = 27% Median Pct Recovery = 27% Median Pct Recovery = 27% Median Pct Recovery = 27% Median Pct Recovery = 27% Median Pct Recovery = 27% Median Pct Recovery = 27% Median Pct Recovery = 27% Median Pct Recovery = 27% Median Pct Recovery = 27% Median Pct Recovery = 27% Median Pct Recovery = 27% Median Pct Recovery = 27% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
TRIS(2-CHLOROETHYL)PHOSPHATE
METHOD: 5433 , TESTIDCODE: 63230GM008
DATES: 11/09/16 - 03/17/17
Open Data Set

Expected Conc. = 802 Median Pct Recovery = 21% Expected Conc. = 802 Median Pct Recovery = 21% Expected Conc. = 802 Median Pct Recovery = 21% Expected Conc. = 505 Median Pct Recovery = 21% Expected Conc. = 505 Median Pct Recovery = 21% Expected Conc. = 505 Median Pct Recovery = 21% Expected Conc. = 505 Median Pct Recovery = 21% Expected Conc. = 500 Median Pct Recovery = 21% Expected Conc. = 500 Median Pct Recovery = 21% Expected Conc. = 500 Median Pct Recovery = 21% Expected Conc. = 500 Median Pct Recovery = 21% Expected Conc. = 500 Median Pct Recovery = 21% Expected Conc. = 500 Median Pct Recovery = 21% Expected Conc. = 500 Median Pct Recovery = 21% Expected Conc. = 500 Median Pct Recovery = 21% Expected Conc. = 500 Median Pct Recovery = 21% Expected Conc. = 500 Median Pct Recovery = 21% Expected Conc. = 500 Median Pct Recovery = 21% Expected Conc. = 500 Median Pct Recovery = 21% Expected Conc. = 802 Median Pct Recovery = 21% Expected Conc. = 802 Median Pct Recovery = 21% Expected Conc. = 505 Median Pct Recovery = 21% Analysis Date = 03/15/17 SpikeMix = ERA 04121605: 0 µl & Abs 051816sed3H1: 0 µl Pct Recovery = 12% Analysis Date = 11/10/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 051816sed3H1: 0 µl Pct Recovery = 1% Analysis Date = 11/09/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 051816sed3L1: 0 µl Pct Recovery = 5% Analysis Date = 11/09/16 SpikeMix = Abs 051816sed3L1: 0 µl & Abs 050916sed3L2: 0 µl Pct Recovery = 6% Analysis Date = 03/17/17 SpikeMix = Abs 050916sed3L3: 0 µl & ERA 04121604: 0 µl Pct Recovery = 10% Analysis Date = 03/17/17 SpikeMix = ERA 04121604: 0 µl & ERA 04121605: 0 µl Pct Recovery = 32% Analysis Date = 03/17/17 SpikeMix = ERA 04121606: 0 µl & ERA 04121604: 0 µl Pct Recovery = 31% Analysis Date = 02/21/17 SpikeMix = ERA 04121606: 0 µl & ERA 04121604: 0 µl Pct Recovery = 36% Analysis Date = 02/21/17 SpikeMix = ERA 04121604: 0 µl & Abs 050916sed3L2: 0 µl Pct Recovery = 33% Analysis Date = 02/10/17 SpikeMix = ERA 04121604: 0 µl & ERA 04121605: 0 µl Pct Recovery = 34% Median Pct Recovery = 21% Median Pct Recovery = 21% Median Pct Recovery = 21% Median Pct Recovery = 21% Median Pct Recovery = 21% Median Pct Recovery = 21% Median Pct Recovery = 21% Median Pct Recovery = 21% Median Pct Recovery = 21% Median Pct Recovery = 21% Median Pct Recovery = 21% Median Pct Recovery = 21% Median Pct Recovery = 21% Median Pct Recovery = 21% Median Pct Recovery = 21% Median Pct Recovery = 21% Median Pct Recovery = 21% Median Pct Recovery = 21% Median Pct Recovery = 21% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
TRIBUTYL PHOSPHATE
METHOD: 5433 , TESTIDCODE: 63231GM008
DATES: 10/12/16 - 03/17/17
Open Data Set

Expected Conc. = 400 Median Pct Recovery = 47% Expected Conc. = 400 Median Pct Recovery = 47% Expected Conc. = 400 Median Pct Recovery = 47% Expected Conc. = 400 Median Pct Recovery = 47% Expected Conc. = 400 Median Pct Recovery = 47% Expected Conc. = 252 Median Pct Recovery = 47% Expected Conc. = 252 Median Pct Recovery = 47% Expected Conc. = 252 Median Pct Recovery = 47% Expected Conc. = 252 Median Pct Recovery = 47% Expected Conc. = 252 Median Pct Recovery = 47% Expected Conc. = 252 Median Pct Recovery = 47% Expected Conc. = 252 Median Pct Recovery = 47% Expected Conc. = 252 Median Pct Recovery = 47% Expected Conc. = 252 Median Pct Recovery = 47% Expected Conc. = 252 Median Pct Recovery = 47% Expected Conc. = 248 Median Pct Recovery = 47% Expected Conc. = 248 Median Pct Recovery = 47% Expected Conc. = 248 Median Pct Recovery = 47% Expected Conc. = 248 Median Pct Recovery = 47% Expected Conc. = 252 Median Pct Recovery = 47% Expected Conc. = 252 Median Pct Recovery = 47% Expected Conc. = 248 Median Pct Recovery = 47% Analysis Date = 11/10/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 051816sed3H1: 0 µl Pct Recovery = 24% Analysis Date = 11/09/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 051816sed3L1: 0 µl Pct Recovery = 47% Analysis Date = 10/12/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 050916sed3H2: 0 µl Pct Recovery = 48% Analysis Date = 03/17/17 SpikeMix = ERA 04121606: 0 µl Pct Recovery = 91% Analysis Date = 03/17/17 SpikeMix = ERA 04121606: 0 µl & ERA 04121604: 0 µl Pct Recovery = 43% Analysis Date = 03/15/17 SpikeMix = ERA 04121605: 0 µl & ERA 04121606: 0 µl Pct Recovery = 44% Analysis Date = 02/21/17 SpikeMix = ERA 04121606: 0 µl & ERA 04121604: 0 µl Pct Recovery = 44% Analysis Date = 02/10/17 SpikeMix = ERA 04121605: 0 µl & ERA 04121606: 0 µl Pct Recovery = 53% Analysis Date = 03/17/17 SpikeMix = Abs 050916sed3L3: 0 µl & ERA 04121604: 0 µl Pct Recovery = 47% Analysis Date = 11/09/16 SpikeMix = Abs 050916sed3H2: 0 µl & Abs 050916sed3L3: 0 µl Pct Recovery = 47% Median Pct Recovery = 47% Median Pct Recovery = 47% Median Pct Recovery = 47% Median Pct Recovery = 47% Median Pct Recovery = 47% Median Pct Recovery = 47% Median Pct Recovery = 47% Median Pct Recovery = 47% Median Pct Recovery = 47% Median Pct Recovery = 47% Median Pct Recovery = 47% Median Pct Recovery = 47% Median Pct Recovery = 47% Median Pct Recovery = 47% Median Pct Recovery = 47% Median Pct Recovery = 47% Median Pct Recovery = 47% Median Pct Recovery = 47% Median Pct Recovery = 47% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
TRICLOSAN
METHOD: 5433 , TESTIDCODE: 63232GM008
DATES: 11/09/16 - 03/17/17
Open Data Set

Expected Conc. = 401 Median Pct Recovery = 36% Expected Conc. = 401 Median Pct Recovery = 36% Expected Conc. = 401 Median Pct Recovery = 36% Expected Conc. = 250 Median Pct Recovery = 36% Expected Conc. = 250 Median Pct Recovery = 36% Expected Conc. = 250 Median Pct Recovery = 36% Expected Conc. = 250 Median Pct Recovery = 36% Expected Conc. = 250 Median Pct Recovery = 36% Expected Conc. = 250 Median Pct Recovery = 36% Expected Conc. = 250 Median Pct Recovery = 36% Expected Conc. = 250 Median Pct Recovery = 36% Expected Conc. = 250 Median Pct Recovery = 36% Expected Conc. = 250 Median Pct Recovery = 36% Expected Conc. = 250 Median Pct Recovery = 36% Expected Conc. = 250 Median Pct Recovery = 36% Expected Conc. = 249 Median Pct Recovery = 36% Expected Conc. = 249 Median Pct Recovery = 36% Expected Conc. = 249 Median Pct Recovery = 36% Expected Conc. = 249 Median Pct Recovery = 36% Expected Conc. = 401 Median Pct Recovery = 36% Expected Conc. = 401 Median Pct Recovery = 36% Expected Conc. = 249 Median Pct Recovery = 36% Analysis Date = 03/15/17 SpikeMix = ERA 04121605: 0 µl & Abs 051816sed3H1: 0 µl Pct Recovery = 35% Analysis Date = 11/10/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 051816sed3H1: 0 µl Pct Recovery = 18% Analysis Date = 03/17/17 SpikeMix = Abs 050916sed3L3: 0 µl & ERA 04121604: 0 µl Pct Recovery = 31% Analysis Date = 03/17/17 SpikeMix = ERA 04121604: 0 µl & ERA 04121605: 0 µl Pct Recovery = 36% Analysis Date = 03/17/17 SpikeMix = ERA 04121606: 0 µl & ERA 04121604: 0 µl Pct Recovery = 34% Analysis Date = 02/21/17 SpikeMix = ERA 04121606: 0 µl & ERA 04121604: 0 µl Pct Recovery = 44% Analysis Date = 02/21/17 SpikeMix = ERA 04121604: 0 µl & Abs 050916sed3L2: 0 µl Pct Recovery = 40% Analysis Date = 02/10/17 SpikeMix = ERA 04121604: 0 µl & ERA 04121605: 0 µl Pct Recovery = 37% Analysis Date = 11/09/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 051816sed3L1: 0 µl Pct Recovery = 46% Analysis Date = 11/09/16 SpikeMix = Abs 051816sed3L1: 0 µl & Abs 050916sed3L2: 0 µl Pct Recovery = 45% Median Pct Recovery = 36% Median Pct Recovery = 36% Median Pct Recovery = 36% Median Pct Recovery = 36% Median Pct Recovery = 36% Median Pct Recovery = 36% Median Pct Recovery = 36% Median Pct Recovery = 36% Median Pct Recovery = 36% Median Pct Recovery = 36% Median Pct Recovery = 36% Median Pct Recovery = 36% Median Pct Recovery = 36% Median Pct Recovery = 36% Median Pct Recovery = 36% Median Pct Recovery = 36% Median Pct Recovery = 36% Median Pct Recovery = 36% Median Pct Recovery = 36% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
TRIPHENYL PHOSPHATE
METHOD: 5433 , TESTIDCODE: 63234GM008
DATES: 10/12/16 - 03/17/17
Open Data Set

Expected Conc. = 401 Median Pct Recovery = 21% Expected Conc. = 401 Median Pct Recovery = 21% Expected Conc. = 401 Median Pct Recovery = 21% Expected Conc. = 401 Median Pct Recovery = 21% Expected Conc. = 401 Median Pct Recovery = 21% Expected Conc. = 253 Median Pct Recovery = 21% Expected Conc. = 253 Median Pct Recovery = 21% Expected Conc. = 253 Median Pct Recovery = 21% Expected Conc. = 253 Median Pct Recovery = 21% Expected Conc. = 253 Median Pct Recovery = 21% Expected Conc. = 253 Median Pct Recovery = 21% Expected Conc. = 253 Median Pct Recovery = 21% Expected Conc. = 253 Median Pct Recovery = 21% Expected Conc. = 253 Median Pct Recovery = 21% Expected Conc. = 253 Median Pct Recovery = 21% Expected Conc. = 249 Median Pct Recovery = 21% Expected Conc. = 249 Median Pct Recovery = 21% Expected Conc. = 249 Median Pct Recovery = 21% Expected Conc. = 249 Median Pct Recovery = 21% Expected Conc. = 253 Median Pct Recovery = 21% Expected Conc. = 253 Median Pct Recovery = 21% Expected Conc. = 249 Median Pct Recovery = 21% Analysis Date = 11/10/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 051816sed3H1: 0 µl Pct Recovery = 2% Analysis Date = 11/09/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 051816sed3L1: 0 µl Pct Recovery = 25% Analysis Date = 10/12/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 050916sed3H2: 0 µl Pct Recovery = 29% Analysis Date = 03/17/17 SpikeMix = ERA 04121606: 0 µl Pct Recovery = 47% Analysis Date = 03/17/17 SpikeMix = ERA 04121606: 0 µl & ERA 04121604: 0 µl Pct Recovery = 22% Analysis Date = 03/15/17 SpikeMix = ERA 04121605: 0 µl & ERA 04121606: 0 µl Pct Recovery = 15% Analysis Date = 02/21/17 SpikeMix = ERA 04121606: 0 µl & ERA 04121604: 0 µl Pct Recovery = 25% Analysis Date = 02/10/17 SpikeMix = ERA 04121605: 0 µl & ERA 04121606: 0 µl Pct Recovery = 21% Analysis Date = 03/17/17 SpikeMix = Abs 050916sed3L3: 0 µl & ERA 04121604: 0 µl Pct Recovery = 18% Analysis Date = 11/09/16 SpikeMix = Abs 050916sed3H2: 0 µl & Abs 050916sed3L3: 0 µl Pct Recovery = 21% Median Pct Recovery = 21% Median Pct Recovery = 21% Median Pct Recovery = 21% Median Pct Recovery = 21% Median Pct Recovery = 21% Median Pct Recovery = 21% Median Pct Recovery = 21% Median Pct Recovery = 21% Median Pct Recovery = 21% Median Pct Recovery = 21% Median Pct Recovery = 21% Median Pct Recovery = 21% Median Pct Recovery = 21% Median Pct Recovery = 21% Median Pct Recovery = 21% Median Pct Recovery = 21% Median Pct Recovery = 21% Median Pct Recovery = 21% Median Pct Recovery = 21% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
TRIS(DICHLORISOPROPYL)PHOSPHATE
METHOD: 5433 , TESTIDCODE: 63235GM008
DATES: 11/09/16 - 03/17/17
Open Data Set

Expected Conc. = 801 Median Pct Recovery = 20% Expected Conc. = 505 Median Pct Recovery = 20% Expected Conc. = 505 Median Pct Recovery = 20% Expected Conc. = 505 Median Pct Recovery = 20% Expected Conc. = 505 Median Pct Recovery = 20% Expected Conc. = 500 Median Pct Recovery = 20% Expected Conc. = 500 Median Pct Recovery = 20% Expected Conc. = 500 Median Pct Recovery = 20% Expected Conc. = 500 Median Pct Recovery = 20% Expected Conc. = 500 Median Pct Recovery = 20% Expected Conc. = 500 Median Pct Recovery = 20% Expected Conc. = 500 Median Pct Recovery = 20% Expected Conc. = 500 Median Pct Recovery = 20% Expected Conc. = 500 Median Pct Recovery = 20% Expected Conc. = 500 Median Pct Recovery = 20% Expected Conc. = 500 Median Pct Recovery = 20% Expected Conc. = 500 Median Pct Recovery = 20% Expected Conc. = 801 Median Pct Recovery = 20% Expected Conc. = 801 Median Pct Recovery = 20% Expected Conc. = 801 Median Pct Recovery = 20% Expected Conc. = 801 Median Pct Recovery = 20% Expected Conc. = 505 Median Pct Recovery = 20% Analysis Date = 03/15/17 SpikeMix = ERA 04121605: 0 µl & Abs 051816sed3H1: 0 µl Pct Recovery = 15% Analysis Date = 11/09/16 SpikeMix = Abs 050916sed3H3: 0 µl & Abs 051816sed3L1: 0 µl Pct Recovery = 21% Analysis Date = 11/09/16 SpikeMix = Abs 051816sed3L1: 0 µl & Abs 050916sed3L2: 0 µl Pct Recovery = 26% Analysis Date = 03/17/17 SpikeMix = Abs 050916sed3L3: 0 µl & ERA 04121604: 0 µl Pct Recovery = 14% Analysis Date = 03/17/17 SpikeMix = ERA 04121604: 0 µl & ERA 04121605: 0 µl Pct Recovery = 20% Analysis Date = 03/17/17 SpikeMix = ERA 04121606: 0 µl & ERA 04121604: 0 µl Pct Recovery = 19% Analysis Date = 02/21/17 SpikeMix = ERA 04121606: 0 µl & ERA 04121604: 0 µl Pct Recovery = 27% Analysis Date = 02/21/17 SpikeMix = ERA 04121604: 0 µl & Abs 050916sed3L2: 0 µl Pct Recovery = 29% Analysis Date = 02/10/17 SpikeMix = ERA 04121604: 0 µl & ERA 04121605: 0 µl Pct Recovery = 20% Median Pct Recovery = 20% Median Pct Recovery = 20% Median Pct Recovery = 20% Median Pct Recovery = 20% Median Pct Recovery = 20% Median Pct Recovery = 20% Median Pct Recovery = 20% Median Pct Recovery = 20% Median Pct Recovery = 20% Median Pct Recovery = 20% Median Pct Recovery = 20% Median Pct Recovery = 20% Median Pct Recovery = 20% Median Pct Recovery = 20% Median Pct Recovery = 20% Median Pct Recovery = 20% Median Pct Recovery = 20% Median Pct Recovery = 20% Median Pct Recovery = 20% Y = 1
The SGPlot Procedure