BQS Organic Blind Sample Program
False Positives & False Negatives
FIPRONIL
Method: 2033 Testid: 62166GCM29
Open Data Set

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newdate = 03/02/16 falseneg = -0.01 newdate = 09/13/11 falseneg = -0.01 newdate = 12/03/11 falsepos = 0.0058 newdate = 10/25/11 falsepos = 0.0048 newdate = 02/28/11 falsepos = 0.0044 newdate = 12/20/16 CENC_VAL = 0.043 newdate = 09/14/16 CENC_VAL = 0.045 newdate = 09/01/16 CENC_VAL = 0.057 newdate = 08/27/16 CENC_VAL = 0.085 newdate = 05/28/16 CENC_VAL = 0.061 newdate = 05/26/16 CENC_VAL = 0.055 newdate = 05/04/16 CENC_VAL = 0.033 newdate = 04/07/16 CENC_VAL = 0.060 newdate = 04/06/16 CENC_VAL = 0.032 newdate = 02/09/16 CENC_VAL = 0.033 newdate = 02/08/16 CENC_VAL = 0.057 newdate = 02/02/16 CENC_VAL = 0.029 newdate = 01/28/16 CENC_VAL = 0.018 newdate = 01/21/16 CENC_VAL = 0.095 newdate = 09/17/15 CENC_VAL = 0.095 newdate = 09/05/15 CENC_VAL = 0.047 newdate = 07/31/15 CENC_VAL = 0.033 newdate = 07/21/15 CENC_VAL = 0.060 newdate = 07/10/15 CENC_VAL = 0.036 newdate = 05/12/15 CENC_VAL = 0.049 newdate = 05/12/15 CENC_VAL = 0.030 newdate = 02/21/15 CENC_VAL = 0.076 newdate = 01/31/15 CENC_VAL = 0.050 newdate = 12/04/14 CENC_VAL = 0.073 newdate = 11/19/14 CENC_VAL = 0.067 newdate = 10/21/14 CENC_VAL = 0.042 newdate = 10/04/14 CENC_VAL = 0.073 newdate = 09/22/14 CENC_VAL = 0.044 newdate = 08/27/14 CENC_VAL = 0.064 newdate = 07/17/14 CENC_VAL = 0.034 newdate = 07/09/14 CENC_VAL = 0.072 newdate = 06/30/14 CENC_VAL = 0.033 newdate = 06/26/14 CENC_VAL = 0.043 newdate = 05/28/14 CENC_VAL = 0.032 newdate = 05/20/14 CENC_VAL = 0.069 newdate = 04/29/14 CENC_VAL = 0.039 newdate = 03/05/14 CENC_VAL = 0.046 newdate = 02/12/14 CENC_VAL = 0.095 newdate = 01/10/14 CENC_VAL = 0.039 newdate = 01/08/14 CENC_VAL = 0.048 newdate = 11/23/13 CENC_VAL = 0.076 newdate = 11/09/13 CENC_VAL = 0.054 newdate = 09/24/13 CENC_VAL = 0.117 newdate = 09/20/13 CENC_VAL = 0.220 newdate = 08/19/13 CENC_VAL = 0.126 newdate = 07/11/13 CENC_VAL = 0.024 newdate = 06/11/13 CENC_VAL = 0.051 newdate = 06/05/13 CENC_VAL = 0.142 newdate = 04/22/13 CENC_VAL = 0.081 newdate = 04/02/13 CENC_VAL = 0.078 newdate = 03/07/13 CENC_VAL = 0.038 newdate = 02/22/13 CENC_VAL = 0.033 newdate = 01/17/13 CENC_VAL = 0.078 newdate = 01/15/13 CENC_VAL = 0.063 newdate = 12/06/12 CENC_VAL = 0.136 newdate = 11/20/12 CENC_VAL = 0.128 newdate = 10/18/12 CENC_VAL = 0.074 newdate = 10/12/12 CENC_VAL = 0.082 newdate = 09/17/12 CENC_VAL = 0.035 newdate = 09/05/12 CENC_VAL = 0.037 newdate = 08/14/12 CENC_VAL = 0.045 newdate = 07/14/12 CENC_VAL = 0.042 newdate = 05/15/12 CENC_VAL = 0.164 newdate = 03/09/12 CENC_VAL = 0.087 newdate = 02/14/12 CENC_VAL = 0.096 newdate = 12/22/11 CENC_VAL = 0.088 newdate = 12/04/11 CENC_VAL = 0.074 newdate = 12/03/11 CENC_VAL = 0.006 newdate = 11/17/11 CENC_VAL = 0.130 newdate = 11/01/11 CENC_VAL = 0.132 newdate = 10/25/11 CENC_VAL = 0.005 newdate = 10/02/11 CENC_VAL = 0.115 newdate = 09/24/11 CENC_VAL = 0.092 newdate = 09/13/11 CENC_VAL = 0.093 newdate = 09/01/11 CENC_VAL = 0.121 newdate = 08/17/11 CENC_VAL = 0.102 newdate = 07/20/11 CENC_VAL = 0.085 newdate = 07/14/11 CENC_VAL = 0.121 newdate = 06/22/11 CENC_VAL = 0.073 newdate = 06/20/11 CENC_VAL = 0.172 newdate = 05/25/11 CENC_VAL = 0.084 newdate = 04/23/11 CENC_VAL = 0.081 newdate = 04/20/11 CENC_VAL = 0.083 newdate = 03/30/11 CENC_VAL = 0.067 newdate = 03/08/11 CENC_VAL = 0.091 newdate = 03/05/11 CENC_VAL = 0.038 newdate = 02/28/11 CENC_VAL = 0.004 newdate = 02/09/11 CENC_VAL = 0.131 newdate = 12/20/16 REPORTING LEVEL = 0.018 newdate = 09/14/16 REPORTING LEVEL = 0.018 newdate = 09/14/16 REPORTING LEVEL = 0.018 newdate = 09/01/16 REPORTING LEVEL = 0.018 newdate = 09/01/16 REPORTING LEVEL = 0.018 newdate = 08/27/16 REPORTING LEVEL = 0.018 newdate = 08/27/16 REPORTING LEVEL = 0.018 newdate = 05/28/16 REPORTING LEVEL = 0.018 newdate = 05/28/16 REPORTING LEVEL = 0.018 newdate = 05/26/16 REPORTING LEVEL = 0.018 newdate = 05/26/16 REPORTING LEVEL = 0.018 newdate = 05/04/16 REPORTING LEVEL = 0.018 newdate = 05/04/16 REPORTING LEVEL = 0.018 newdate = 04/07/16 REPORTING LEVEL = 0.018 newdate = 04/07/16 REPORTING LEVEL = 0.018 newdate = 04/06/16 REPORTING LEVEL = 0.018 newdate = 04/06/16 REPORTING LEVEL = 0.018 newdate = 03/02/16 REPORTING LEVEL = 0.018 newdate = 03/02/16 REPORTING LEVEL = 0.018 newdate = 02/09/16 REPORTING LEVEL = 0.018 newdate = 02/09/16 REPORTING LEVEL = 0.018 newdate = 02/08/16 REPORTING LEVEL = 0.018 newdate = 02/08/16 REPORTING LEVEL = 0.018 newdate = 02/02/16 REPORTING LEVEL = 0.018 newdate = 02/02/16 REPORTING LEVEL = 0.018 newdate = 01/28/16 REPORTING LEVEL = 0.018 newdate = 01/28/16 REPORTING LEVEL = 0.018 newdate = 01/21/16 REPORTING LEVEL = 0.018 newdate = 01/21/16 REPORTING LEVEL = 0.018 newdate = 09/17/15 REPORTING LEVEL = 0.018 newdate = 09/17/15 REPORTING LEVEL = 0.018 newdate = 09/05/15 REPORTING LEVEL = 0.018 newdate = 09/05/15 REPORTING LEVEL = 0.018 newdate = 07/31/15 REPORTING LEVEL = 0.018 newdate = 07/31/15 REPORTING LEVEL = 0.018 newdate = 07/21/15 REPORTING LEVEL = 0.018 newdate = 07/21/15 REPORTING LEVEL = 0.018 newdate = 07/10/15 REPORTING LEVEL = 0.018 newdate = 07/10/15 REPORTING LEVEL = 0.018 newdate = 05/12/15 REPORTING LEVEL = 0.018 newdate = 05/12/15 REPORTING LEVEL = 0.018 newdate = 05/12/15 REPORTING LEVEL = 0.018 newdate = 05/12/15 REPORTING LEVEL = 0.018 newdate = 02/21/15 REPORTING LEVEL = 0.018 newdate = 02/21/15 REPORTING LEVEL = 0.018 newdate = 01/31/15 REPORTING LEVEL = 0.018 newdate = 01/31/15 REPORTING LEVEL = 0.018 newdate = 12/04/14 REPORTING LEVEL = 0.018 newdate = 12/04/14 REPORTING LEVEL = 0.018 newdate = 11/19/14 REPORTING LEVEL = 0.018 newdate = 11/19/14 REPORTING LEVEL = 0.018 newdate = 10/21/14 REPORTING LEVEL = 0.018 newdate = 10/21/14 REPORTING LEVEL = 0.018 newdate = 10/04/14 REPORTING LEVEL = 0.018 newdate = 10/04/14 REPORTING LEVEL = 0.018 newdate = 09/22/14 REPORTING LEVEL = 0.018 newdate = 09/22/14 REPORTING LEVEL = 0.018 newdate = 08/27/14 REPORTING LEVEL = 0.018 newdate = 08/27/14 REPORTING LEVEL = 0.018 newdate = 07/17/14 REPORTING LEVEL = 0.018 newdate = 07/17/14 REPORTING LEVEL = 0.018 newdate = 07/09/14 REPORTING LEVEL = 0.018 newdate = 07/09/14 REPORTING LEVEL = 0.018 newdate = 06/30/14 REPORTING LEVEL = 0.018 newdate = 06/30/14 REPORTING LEVEL = 0.018 newdate = 06/26/14 REPORTING LEVEL = 0.018 newdate = 06/26/14 REPORTING LEVEL = 0.018 newdate = 05/28/14 REPORTING LEVEL = 0.018 newdate = 05/28/14 REPORTING LEVEL = 0.018 newdate = 05/20/14 REPORTING LEVEL = 0.018 newdate = 05/20/14 REPORTING LEVEL = 0.018 newdate = 04/29/14 REPORTING LEVEL = 0.018 newdate = 04/29/14 REPORTING LEVEL = 0.018 newdate = 03/05/14 REPORTING LEVEL = 0.018 newdate = 03/05/14 REPORTING LEVEL = 0.018 newdate = 02/12/14 REPORTING LEVEL = 0.018 newdate = 02/12/14 REPORTING LEVEL = 0.018 newdate = 01/10/14 REPORTING LEVEL = 0.018 newdate = 01/10/14 REPORTING LEVEL = 0.018 newdate = 01/08/14 REPORTING LEVEL = 0.018 newdate = 01/08/14 REPORTING LEVEL = 0.018 newdate = 11/23/13 REPORTING LEVEL = 0.018 newdate = 11/23/13 REPORTING LEVEL = 0.018 newdate = 11/09/13 REPORTING LEVEL = 0.018 newdate = 11/09/13 REPORTING LEVEL = 0.018 newdate = 09/24/13 REPORTING LEVEL = 0.018 newdate = 09/24/13 REPORTING LEVEL = 0.018 newdate = 09/20/13 REPORTING LEVEL = 0.018 newdate = 09/20/13 REPORTING LEVEL = 0.018 newdate = 08/19/13 REPORTING LEVEL = 0.018 newdate = 08/19/13 REPORTING LEVEL = 0.018 newdate = 07/11/13 REPORTING LEVEL = 0.018 newdate = 07/11/13 REPORTING LEVEL = 0.018 newdate = 06/11/13 REPORTING LEVEL = 0.018 newdate = 06/11/13 REPORTING LEVEL = 0.018 newdate = 06/05/13 REPORTING LEVEL = 0.018 newdate = 06/05/13 REPORTING LEVEL = 0.018 newdate = 04/22/13 REPORTING LEVEL = 0.018 newdate = 04/22/13 REPORTING LEVEL = 0.018 newdate = 04/02/13 REPORTING LEVEL = 0.018 newdate = 04/02/13 REPORTING LEVEL = 0.018 newdate = 03/07/13 REPORTING LEVEL = 0.018 newdate = 03/07/13 REPORTING LEVEL = 0.018 newdate = 02/22/13 REPORTING LEVEL = 0.018 newdate = 02/22/13 REPORTING LEVEL = 0.018 newdate = 01/17/13 REPORTING LEVEL = 0.018 newdate = 01/17/13 REPORTING LEVEL = 0.018 newdate = 01/15/13 REPORTING LEVEL = 0.018 newdate = 01/15/13 REPORTING LEVEL = 0.018 newdate = 12/06/12 REPORTING LEVEL = 0.018 newdate = 12/06/12 REPORTING LEVEL = 0.018 newdate = 11/20/12 REPORTING LEVEL = 0.018 newdate = 11/20/12 REPORTING LEVEL = 0.018 newdate = 10/18/12 REPORTING LEVEL = 0.018 newdate = 10/18/12 REPORTING LEVEL = 0.018 newdate = 10/12/12 REPORTING LEVEL = 0.018 newdate = 10/12/12 REPORTING LEVEL = 0.018 newdate = 09/17/12 REPORTING LEVEL = 0.018 newdate = 09/17/12 REPORTING LEVEL = 0.018 newdate = 09/05/12 REPORTING LEVEL = 0.018 newdate = 09/05/12 REPORTING LEVEL = 0.018 newdate = 08/14/12 REPORTING LEVEL = 0.018 newdate = 08/14/12 REPORTING LEVEL = 0.018 newdate = 07/14/12 REPORTING LEVEL = 0.018 newdate = 07/14/12 REPORTING LEVEL = 0.018 newdate = 05/15/12 REPORTING LEVEL = 0.018 newdate = 05/15/12 REPORTING LEVEL = 0.018 newdate = 03/09/12 REPORTING LEVEL = 0.018 newdate = 03/09/12 REPORTING LEVEL = 0.018 newdate = 02/14/12 REPORTING LEVEL = 0.018 newdate = 02/14/12 REPORTING LEVEL = 0.018 newdate = 12/22/11 REPORTING LEVEL = 0.018 newdate = 12/22/11 REPORTING LEVEL = 0.018 newdate = 12/04/11 REPORTING LEVEL = 0.018 newdate = 12/04/11 REPORTING LEVEL = 0.018 newdate = 12/03/11 REPORTING LEVEL = 0.018 newdate = 12/03/11 REPORTING LEVEL = 0.018 newdate = 11/17/11 REPORTING LEVEL = 0.018 newdate = 11/17/11 REPORTING LEVEL = 0.018 newdate = 11/01/11 REPORTING LEVEL = 0.018 newdate = 11/01/11 REPORTING LEVEL = 0.018 newdate = 10/25/11 REPORTING LEVEL = 0.018 newdate = 10/25/11 REPORTING LEVEL = 0.018 newdate = 10/02/11 REPORTING LEVEL = 0.018 newdate = 10/02/11 REPORTING LEVEL = 0.018 newdate = 09/24/11 REPORTING LEVEL = 0.018 newdate = 09/24/11 REPORTING LEVEL = 0.018 newdate = 09/13/11 REPORTING LEVEL = 0.018 newdate = 09/13/11 REPORTING LEVEL = 0.018 newdate = 09/13/11 REPORTING LEVEL = 0.018 newdate = 09/13/11 REPORTING LEVEL = 0.018 newdate = 09/01/11 REPORTING LEVEL = 0.018 newdate = 09/01/11 REPORTING LEVEL = 0.018 newdate = 08/17/11 REPORTING LEVEL = 0.018 newdate = 08/17/11 REPORTING LEVEL = 0.018 newdate = 07/20/11 REPORTING LEVEL = 0.018 newdate = 07/20/11 REPORTING LEVEL = 0.018 newdate = 07/14/11 REPORTING LEVEL = 0.018 newdate = 07/14/11 REPORTING LEVEL = 0.018 newdate = 06/22/11 REPORTING LEVEL = 0.018 newdate = 06/22/11 REPORTING LEVEL = 0.018 newdate = 06/20/11 REPORTING LEVEL = 0.018 newdate = 06/20/11 REPORTING LEVEL = 0.018 newdate = 05/25/11 REPORTING LEVEL = 0.018 newdate = 05/25/11 REPORTING LEVEL = 0.018 newdate = 04/23/11 REPORTING LEVEL = 0.018 newdate = 04/23/11 REPORTING LEVEL = 0.018 newdate = 04/20/11 REPORTING LEVEL = 0.018 newdate = 04/20/11 REPORTING LEVEL = 0.018 newdate = 03/30/11 REPORTING LEVEL = 0.018 newdate = 03/30/11 REPORTING LEVEL = 0.018 newdate = 03/08/11 REPORTING LEVEL = 0.018 newdate = 03/08/11 REPORTING LEVEL = 0.018 newdate = 03/05/11 REPORTING LEVEL = 0.018 newdate = 03/05/11 REPORTING LEVEL = 0.018 newdate = 02/28/11 REPORTING LEVEL = 0.018 newdate = 02/28/11 REPORTING LEVEL = 0.018 newdate = 02/09/11 REPORTING LEVEL = 0.018 Y = 0
The SGPlot Procedure

Updated 07/06/2017

False Positive & Negative Listing for FIPRONIL

Status Lab ID Spike Mix Reporting Level Analysis Date Result Conc. Expected Conc.
False Negative 20112310030 ERA 0318-13-02.2: 40 µl 0.018 09/13/11 < 0.018 0.0996
  20160210080 Abs 041415: 20 µl & ChemService 3851600: 20 µl 0.018 03/02/16 < 0.0242 0.027
False Positive 20110410061 ERA 0818-10-05 LS 2033#2: 80 µl 0.018 02/28/11 E 0.0044 0
  20112870073 ERA 0818-10-05 LS 2033#2: 40 µl 0.018 10/25/11 E 0.0048 0
  20113220198 ERA 0818-10-05 LS 2033#2: 80 µl 0.018 12/03/11 E 0.0058 0

Updated 07/06/2017