BQS Organic Blind Sample Program
False Positives & False Negatives
AZINPHOS-METHYL-OXON
Method: 2033 Testid: 61635GCM39
Open Data Set

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newdate = 09/20/16 falseneg = -0.01 newdate = 09/09/16 falseneg = -0.01 newdate = 07/31/15 falseneg = -0.01 newdate = 07/16/14 falseneg = -0.01 newdate = 05/28/14 falseneg = -0.01 newdate = 04/03/14 falseneg = -0.01 newdate = 03/05/14 falseneg = -0.01 newdate = 09/24/13 falseneg = -0.01 newdate = 08/19/13 falseneg = -0.01 newdate = 09/26/12 falseneg = -0.01 newdate = 08/14/12 falseneg = -0.01 newdate = 06/22/11 falseneg = -0.01 newdate = 09/01/16 falsepos = 0.207 newdate = 09/01/16 CENC_VAL = 0.207 newdate = 08/27/16 CENC_VAL = 0.138 newdate = 05/04/16 CENC_VAL = 0.064 newdate = 04/06/16 CENC_VAL = 0.071 newdate = 03/02/16 CENC_VAL = 0.041 newdate = 01/28/16 CENC_VAL = 0.039 newdate = 09/05/15 CENC_VAL = 0.096 newdate = 07/21/15 CENC_VAL = 0.101 newdate = 05/12/15 CENC_VAL = 0.076 newdate = 05/12/15 CENC_VAL = 0.034 newdate = 03/31/15 CENC_VAL = 0.045 newdate = 07/09/14 CENC_VAL = 0.092 newdate = 06/28/14 CENC_VAL = 0.086 newdate = 06/26/14 CENC_VAL = 0.060 newdate = 06/24/14 CENC_VAL = 0.033 newdate = 04/15/14 CENC_VAL = 0.072 newdate = 01/31/14 CENC_VAL = 0.161 newdate = 01/18/14 CENC_VAL = 0.235 newdate = 01/10/14 CENC_VAL = 0.057 newdate = 01/08/14 CENC_VAL = 0.074 newdate = 12/05/13 CENC_VAL = 0.079 newdate = 11/23/13 CENC_VAL = 0.055 newdate = 11/04/13 CENC_VAL = 0.040 newdate = 10/19/13 CENC_VAL = 0.112 newdate = 09/14/13 CENC_VAL = 0.140 newdate = 09/05/13 CENC_VAL = 0.064 newdate = 07/23/13 CENC_VAL = 0.065 newdate = 06/26/13 CENC_VAL = 0.064 newdate = 06/11/13 CENC_VAL = 0.069 newdate = 05/22/13 CENC_VAL = 0.079 newdate = 04/22/13 CENC_VAL = 0.145 newdate = 03/18/13 CENC_VAL = 0.054 newdate = 03/07/13 CENC_VAL = 0.131 newdate = 02/06/13 CENC_VAL = 0.318 newdate = 01/17/13 CENC_VAL = 0.219 newdate = 01/15/13 CENC_VAL = 0.157 newdate = 12/20/12 CENC_VAL = 0.289 newdate = 12/06/12 CENC_VAL = 0.722 newdate = 11/14/12 CENC_VAL = 0.215 newdate = 10/18/12 CENC_VAL = 0.160 newdate = 10/12/12 CENC_VAL = 0.131 newdate = 09/17/12 CENC_VAL = 0.129 newdate = 09/05/12 CENC_VAL = 0.028 newdate = 08/29/12 CENC_VAL = 0.105 newdate = 06/16/12 CENC_VAL = 0.172 newdate = 04/20/11 CENC_VAL = 0.074 newdate = 03/05/11 CENC_VAL = 0.042 newdate = 09/20/16 REPORTING LEVEL = 0.042 newdate = 09/09/16 REPORTING LEVEL = 0.042 newdate = 09/09/16 REPORTING LEVEL = 0.042 newdate = 09/01/16 REPORTING LEVEL = 0.042 newdate = 09/01/16 REPORTING LEVEL = 0.042 newdate = 08/27/16 REPORTING LEVEL = 0.042 newdate = 08/27/16 REPORTING LEVEL = 0.042 newdate = 05/04/16 REPORTING LEVEL = 0.042 newdate = 05/04/16 REPORTING LEVEL = 0.042 newdate = 04/06/16 REPORTING LEVEL = 0.042 newdate = 04/06/16 REPORTING LEVEL = 0.042 newdate = 03/02/16 REPORTING LEVEL = 0.042 newdate = 03/02/16 REPORTING LEVEL = 0.042 newdate = 02/02/16 REPORTING LEVEL = 0.042 newdate = 02/02/16 REPORTING LEVEL = 0.042 newdate = 01/28/16 REPORTING LEVEL = 0.042 newdate = 01/28/16 REPORTING LEVEL = 0.042 newdate = 09/05/15 REPORTING LEVEL = 0.042 newdate = 09/05/15 REPORTING LEVEL = 0.042 newdate = 07/31/15 REPORTING LEVEL = 0.042 newdate = 07/31/15 REPORTING LEVEL = 0.042 newdate = 07/21/15 REPORTING LEVEL = 0.042 newdate = 07/21/15 REPORTING LEVEL = 0.042 newdate = 05/12/15 REPORTING LEVEL = 0.042 newdate = 05/12/15 REPORTING LEVEL = 0.042 newdate = 05/12/15 REPORTING LEVEL = 0.042 newdate = 05/12/15 REPORTING LEVEL = 0.042 newdate = 03/31/15 REPORTING LEVEL = 0.042 newdate = 03/31/15 REPORTING LEVEL = 0.042 newdate = 07/16/14 REPORTING LEVEL = 0.042 newdate = 07/16/14 REPORTING LEVEL = 0.042 newdate = 07/09/14 REPORTING LEVEL = 0.042 newdate = 07/09/14 REPORTING LEVEL = 0.042 newdate = 06/28/14 REPORTING LEVEL = 0.042 newdate = 06/28/14 REPORTING LEVEL = 0.042 newdate = 06/26/14 REPORTING LEVEL = 0.042 newdate = 06/26/14 REPORTING LEVEL = 0.042 newdate = 06/24/14 REPORTING LEVEL = 0.042 newdate = 06/24/14 REPORTING LEVEL = 0.042 newdate = 05/28/14 REPORTING LEVEL = 0.042 newdate = 05/28/14 REPORTING LEVEL = 0.042 newdate = 04/15/14 REPORTING LEVEL = 0.042 newdate = 04/15/14 REPORTING LEVEL = 0.042 newdate = 04/03/14 REPORTING LEVEL = 0.042 newdate = 04/03/14 REPORTING LEVEL = 0.042 newdate = 03/05/14 REPORTING LEVEL = 0.042 newdate = 03/05/14 REPORTING LEVEL = 0.042 newdate = 01/31/14 REPORTING LEVEL = 0.042 newdate = 01/31/14 REPORTING LEVEL = 0.042 newdate = 01/18/14 REPORTING LEVEL = 0.042 newdate = 01/18/14 REPORTING LEVEL = 0.042 newdate = 01/10/14 REPORTING LEVEL = 0.042 newdate = 01/10/14 REPORTING LEVEL = 0.042 newdate = 01/08/14 REPORTING LEVEL = 0.042 newdate = 01/08/14 REPORTING LEVEL = 0.042 newdate = 12/05/13 REPORTING LEVEL = 0.042 newdate = 12/05/13 REPORTING LEVEL = 0.042 newdate = 11/23/13 REPORTING LEVEL = 0.042 newdate = 11/23/13 REPORTING LEVEL = 0.042 newdate = 11/04/13 REPORTING LEVEL = 0.042 newdate = 11/04/13 REPORTING LEVEL = 0.042 newdate = 10/19/13 REPORTING LEVEL = 0.042 newdate = 10/19/13 REPORTING LEVEL = 0.042 newdate = 09/24/13 REPORTING LEVEL = 0.042 newdate = 09/24/13 REPORTING LEVEL = 0.042 newdate = 09/14/13 REPORTING LEVEL = 0.042 newdate = 09/14/13 REPORTING LEVEL = 0.042 newdate = 09/05/13 REPORTING LEVEL = 0.042 newdate = 09/05/13 REPORTING LEVEL = 0.042 newdate = 08/19/13 REPORTING LEVEL = 0.042 newdate = 08/19/13 REPORTING LEVEL = 0.042 newdate = 07/23/13 REPORTING LEVEL = 0.042 newdate = 07/23/13 REPORTING LEVEL = 0.042 newdate = 06/26/13 REPORTING LEVEL = 0.042 newdate = 06/26/13 REPORTING LEVEL = 0.042 newdate = 06/11/13 REPORTING LEVEL = 0.042 newdate = 06/11/13 REPORTING LEVEL = 0.042 newdate = 05/22/13 REPORTING LEVEL = 0.042 newdate = 05/22/13 REPORTING LEVEL = 0.042 newdate = 04/22/13 REPORTING LEVEL = 0.042 newdate = 04/22/13 REPORTING LEVEL = 0.042 newdate = 03/18/13 REPORTING LEVEL = 0.042 newdate = 03/18/13 REPORTING LEVEL = 0.042 newdate = 03/07/13 REPORTING LEVEL = 0.042 newdate = 03/07/13 REPORTING LEVEL = 0.042 newdate = 02/06/13 REPORTING LEVEL = 0.042 newdate = 02/06/13 REPORTING LEVEL = 0.042 newdate = 01/17/13 REPORTING LEVEL = 0.042 newdate = 01/17/13 REPORTING LEVEL = 0.042 newdate = 01/15/13 REPORTING LEVEL = 0.042 newdate = 01/15/13 REPORTING LEVEL = 0.042 newdate = 12/20/12 REPORTING LEVEL = 0.042 newdate = 12/20/12 REPORTING LEVEL = 0.042 newdate = 12/06/12 REPORTING LEVEL = 0.042 newdate = 12/06/12 REPORTING LEVEL = 0.042 newdate = 11/14/12 REPORTING LEVEL = 0.042 newdate = 11/14/12 REPORTING LEVEL = 0.042 newdate = 10/18/12 REPORTING LEVEL = 0.042 newdate = 10/18/12 REPORTING LEVEL = 0.042 newdate = 10/12/12 REPORTING LEVEL = 0.042 newdate = 10/12/12 REPORTING LEVEL = 0.042 newdate = 09/26/12 REPORTING LEVEL = 0.042 newdate = 09/26/12 REPORTING LEVEL = 0.042 newdate = 09/17/12 REPORTING LEVEL = 0.042 newdate = 09/17/12 REPORTING LEVEL = 0.042 newdate = 09/05/12 REPORTING LEVEL = 0.042 newdate = 09/05/12 REPORTING LEVEL = 0.042 newdate = 08/29/12 REPORTING LEVEL = 0.042 newdate = 08/29/12 REPORTING LEVEL = 0.042 newdate = 08/14/12 REPORTING LEVEL = 0.042 newdate = 08/14/12 REPORTING LEVEL = 0.042 newdate = 06/16/12 REPORTING LEVEL = 0.042 newdate = 06/16/12 REPORTING LEVEL = 0.042 newdate = 06/22/11 REPORTING LEVEL = 0.042 newdate = 06/22/11 REPORTING LEVEL = 0.042 newdate = 04/20/11 REPORTING LEVEL = 0.042 newdate = 04/20/11 REPORTING LEVEL = 0.042 newdate = 03/05/11 REPORTING LEVEL = 0.042 Y = 0
The SGPlot Procedure

Updated 07/06/2017

False Positive & Negative Listing for AZINPHOS-METHYL-OXON

Status Lab ID Spike Mix Reporting Level Analysis Date Result Conc. Expected Conc.
False Negative 20111590005 NWQL PSP2SP117A: 75 µl 0.042 06/22/11 < 0.042 0.074096
  20122020004 Abs 052412: 20 µl & Supelco LB92783: 20 µl 0.042 08/14/12 < 0.042 0.1
  20122570122 Restek A088380: 20 µl & Abs 052412: 20 µl 0.042 09/26/12 < 0.042 0.1
  20132140002 Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl 0.042 08/19/13 < 0.042 0.1745
  20132560001 ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl 0.042 09/24/13 < 0.042 0.176
  20140510043 Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl 0.042 03/05/14 < 0.042 0.0698
  20140730138 Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl 0.042 04/03/14 < 0.042 0.0698
  20141360094 Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl 0.042 05/28/14 < 0.042 0.0849
  20141840097 ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl 0.042 07/16/14 < 0.042 0.0849
  20152040177 Abs 041415: 20 µl & ERA 0406-15-01: 20 µl 0.042 07/31/15 < 0.06 0.063
  20161880109 Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl 0.042 09/09/16 < 0.042 0.27
  20162150213 Phenova B20160331: 40 µl & ChemService 5054800: 40 µl 0.042 09/20/16 < 0.0428 0.108
False Positive 20161600087 NSI 041816: 40 µl & Crescent 03FF076: 40 µl 0.042 09/01/16 E 0.207 0

Updated 07/06/2017