BQS OBSP Determination:
11-KETOTESTOSTERONE
METHOD: 6434 , TESTIDCODE: 64467GM006
Open Data Set

Analysis Date = 09/26/16 SpikeMix = Abs 051616sed4H1: 0 µl & Abs 051616sed4L2: 0 µl Pct Recovery = 81% Analysis Date = 10/20/16 SpikeMix = Abs 051616sed4H3: 0 µl & Abs 051616sed4L: 0 µl Pct Recovery = 98% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
11-KETOTESTOSTERONE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 2 89% 12% 89% 12%
Total 2 89% 12% 89% 12%

Sample Statistics
11-KETOTESTOSTERONE

Characteristic N % % Basis
Plotted 2 33% Spiked
Estimated Values 2 33% Spiked
Deleted Values 1 5% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 6 .  
False Negatives 4 67% 4 out of 6
Not Spiked 13 .  
False Positives 0 0% 0 out of 12

BQS OBSP Determination:
17-ALPHA-ESTRADIOL
METHOD: 6434 , TESTIDCODE: 64468GM006
Open Data Set

Analysis Date = 09/26/16 SpikeMix = Abs 051616sed4H3: 0 µl & Abs 051616sed4H2: 0 µl Pct Recovery = 111% Analysis Date = 09/26/16 SpikeMix = Abs 051616sed4H3: 0 µl & Abs 051616sed4H1: 0 µl Pct Recovery = 75% Analysis Date = 05/09/17 SpikeMix = ERA 04121614: 0 µl & Abs 051616sed4L3: 0 µl Pct Recovery = 58% Analysis Date = 09/26/16 SpikeMix = Abs 051616sed4H2: 0 µl & Abs 051616sed4L3: 0 µl Pct Recovery = 106% Analysis Date = 05/09/17 SpikeMix = ERA 04121615: 0 µl & Abs 051616sed4L: 0 µl Pct Recovery = 60% Analysis Date = 03/17/17 SpikeMix = ERA 04121614: 0 µl & ERA 04121615: 0 µl Pct Recovery = 34% Analysis Date = 05/09/17 Pct Recovery = 59% Analysis Date = 05/07/17 Pct Recovery = 59% Analysis Date = 05/07/17 Pct Recovery = 59% Analysis Date = 05/06/17 Pct Recovery = 58% Analysis Date = 05/06/17 Pct Recovery = 58% Analysis Date = 05/05/17 Pct Recovery = 58% Analysis Date = 05/05/17 Pct Recovery = 58% Analysis Date = 05/04/17 Pct Recovery = 57% Analysis Date = 05/04/17 Pct Recovery = 57% Analysis Date = 05/03/17 Pct Recovery = 57% Analysis Date = 05/03/17 Pct Recovery = 57% Analysis Date = 05/02/17 Pct Recovery = 56% Analysis Date = 05/02/17 Pct Recovery = 56% Analysis Date = 05/01/17 Pct Recovery = 55% Analysis Date = 05/01/17 Pct Recovery = 55% Analysis Date = 04/30/17 Pct Recovery = 55% Analysis Date = 04/30/17 Pct Recovery = 55% Analysis Date = 04/28/17 Pct Recovery = 54% Analysis Date = 04/28/17 Pct Recovery = 54% Analysis Date = 04/27/17 Pct Recovery = 54% Analysis Date = 04/27/17 Pct Recovery = 54% Analysis Date = 04/26/17 Pct Recovery = 53% Analysis Date = 04/26/17 Pct Recovery = 53% Analysis Date = 04/25/17 Pct Recovery = 53% Analysis Date = 04/25/17 Pct Recovery = 53% Analysis Date = 04/24/17 Pct Recovery = 52% Analysis Date = 04/24/17 Pct Recovery = 52% Analysis Date = 04/23/17 Pct Recovery = 52% Analysis Date = 04/23/17 Pct Recovery = 52% Analysis Date = 04/22/17 Pct Recovery = 51% Analysis Date = 04/22/17 Pct Recovery = 51% Analysis Date = 04/21/17 Pct Recovery = 51% Analysis Date = 04/21/17 Pct Recovery = 51% Analysis Date = 04/19/17 Pct Recovery = 50% Analysis Date = 04/19/17 Pct Recovery = 50% Analysis Date = 04/18/17 Pct Recovery = 50% Analysis Date = 04/18/17 Pct Recovery = 50% Analysis Date = 04/17/17 Pct Recovery = 49% Analysis Date = 04/17/17 Pct Recovery = 49% Analysis Date = 04/16/17 Pct Recovery = 49% Analysis Date = 04/16/17 Pct Recovery = 49% Analysis Date = 04/15/17 Pct Recovery = 48% Analysis Date = 04/15/17 Pct Recovery = 48% Analysis Date = 04/14/17 Pct Recovery = 48% Analysis Date = 04/14/17 Pct Recovery = 48% Analysis Date = 04/13/17 Pct Recovery = 47% Analysis Date = 04/13/17 Pct Recovery = 47% Analysis Date = 04/12/17 Pct Recovery = 46% Analysis Date = 04/12/17 Pct Recovery = 46% Analysis Date = 04/10/17 Pct Recovery = 46% Analysis Date = 04/10/17 Pct Recovery = 46% Analysis Date = 04/09/17 Pct Recovery = 45% Analysis Date = 04/09/17 Pct Recovery = 45% Analysis Date = 04/08/17 Pct Recovery = 45% Analysis Date = 04/08/17 Pct Recovery = 45% Analysis Date = 04/07/17 Pct Recovery = 44% Analysis Date = 04/07/17 Pct Recovery = 44% Analysis Date = 04/06/17 Pct Recovery = 44% Analysis Date = 04/06/17 Pct Recovery = 44% Analysis Date = 04/05/17 Pct Recovery = 43% Analysis Date = 04/05/17 Pct Recovery = 43% Analysis Date = 04/04/17 Pct Recovery = 43% Analysis Date = 04/04/17 Pct Recovery = 43% Analysis Date = 04/03/17 Pct Recovery = 42% Analysis Date = 04/03/17 Pct Recovery = 42% Analysis Date = 04/01/17 Pct Recovery = 42% Analysis Date = 04/01/17 Pct Recovery = 42% Analysis Date = 03/31/17 Pct Recovery = 41% Analysis Date = 03/31/17 Pct Recovery = 41% Analysis Date = 03/30/17 Pct Recovery = 41% Analysis Date = 03/30/17 Pct Recovery = 41% Analysis Date = 03/29/17 Pct Recovery = 40% Analysis Date = 03/29/17 Pct Recovery = 40% Analysis Date = 03/28/17 Pct Recovery = 40% Analysis Date = 03/28/17 Pct Recovery = 40% Analysis Date = 03/27/17 Pct Recovery = 39% Analysis Date = 03/27/17 Pct Recovery = 39% Analysis Date = 03/26/17 Pct Recovery = 39% Analysis Date = 03/26/17 Pct Recovery = 39% Analysis Date = 03/25/17 Pct Recovery = 38% Analysis Date = 03/25/17 Pct Recovery = 38% Analysis Date = 03/23/17 Pct Recovery = 37% Analysis Date = 03/23/17 Pct Recovery = 37% Analysis Date = 03/22/17 Pct Recovery = 37% Analysis Date = 03/22/17 Pct Recovery = 37% Analysis Date = 03/21/17 Pct Recovery = 36% Analysis Date = 03/21/17 Pct Recovery = 36% Analysis Date = 03/20/17 Pct Recovery = 36% Analysis Date = 03/20/17 Pct Recovery = 36% Analysis Date = 03/19/17 Pct Recovery = 35% Analysis Date = 03/19/17 Pct Recovery = 35% Analysis Date = 03/18/17 Pct Recovery = 35% Analysis Date = 03/18/17 Pct Recovery = 35% Analysis Date = 03/17/17 Pct Recovery = 34% Analysis Date = 03/17/17 Pct Recovery = 34% Analysis Date = 03/16/17 Pct Recovery = 35% Analysis Date = 03/16/17 Pct Recovery = 35% Analysis Date = 03/14/17 Pct Recovery = 35% Analysis Date = 03/14/17 Pct Recovery = 35% Analysis Date = 03/13/17 Pct Recovery = 35% Analysis Date = 03/13/17 Pct Recovery = 35% Analysis Date = 03/12/17 Pct Recovery = 36% Analysis Date = 03/12/17 Pct Recovery = 36% Analysis Date = 03/11/17 Pct Recovery = 36% Analysis Date = 03/11/17 Pct Recovery = 36% Analysis Date = 03/10/17 Pct Recovery = 37% Analysis Date = 03/10/17 Pct Recovery = 37% Analysis Date = 03/09/17 Pct Recovery = 37% Analysis Date = 03/09/17 Pct Recovery = 37% Analysis Date = 03/08/17 Pct Recovery = 37% Analysis Date = 03/08/17 Pct Recovery = 37% Analysis Date = 03/07/17 Pct Recovery = 38% Analysis Date = 03/07/17 Pct Recovery = 38% Analysis Date = 03/05/17 Pct Recovery = 38% Analysis Date = 03/05/17 Pct Recovery = 38% Analysis Date = 03/04/17 Pct Recovery = 39% Analysis Date = 03/04/17 Pct Recovery = 39% Analysis Date = 03/03/17 Pct Recovery = 39% Analysis Date = 03/03/17 Pct Recovery = 39% Analysis Date = 03/02/17 Pct Recovery = 40% Analysis Date = 03/02/17 Pct Recovery = 40% Analysis Date = 03/01/17 Pct Recovery = 40% Analysis Date = 03/01/17 Pct Recovery = 40% Analysis Date = 02/28/17 Pct Recovery = 40% Analysis Date = 02/28/17 Pct Recovery = 40% Analysis Date = 02/27/17 Pct Recovery = 41% Analysis Date = 02/27/17 Pct Recovery = 41% Analysis Date = 02/26/17 Pct Recovery = 41% Analysis Date = 02/26/17 Pct Recovery = 41% Analysis Date = 02/24/17 Pct Recovery = 42% Analysis Date = 02/24/17 Pct Recovery = 42% Analysis Date = 02/23/17 Pct Recovery = 42% Analysis Date = 02/23/17 Pct Recovery = 42% Analysis Date = 02/22/17 Pct Recovery = 42% Analysis Date = 02/22/17 Pct Recovery = 42% Analysis Date = 02/21/17 Pct Recovery = 43% Analysis Date = 02/21/17 Pct Recovery = 43% Analysis Date = 02/20/17 Pct Recovery = 43% Analysis Date = 02/20/17 Pct Recovery = 43% Analysis Date = 02/19/17 Pct Recovery = 44% Analysis Date = 02/19/17 Pct Recovery = 44% Analysis Date = 02/18/17 Pct Recovery = 44% Analysis Date = 02/18/17 Pct Recovery = 44% Analysis Date = 02/17/17 Pct Recovery = 44% Analysis Date = 02/17/17 Pct Recovery = 44% Analysis Date = 02/15/17 Pct Recovery = 45% Analysis Date = 02/15/17 Pct Recovery = 45% Analysis Date = 02/14/17 Pct Recovery = 45% Analysis Date = 02/14/17 Pct Recovery = 45% Analysis Date = 02/13/17 Pct Recovery = 46% Analysis Date = 02/13/17 Pct Recovery = 46% Analysis Date = 02/12/17 Pct Recovery = 46% Analysis Date = 02/12/17 Pct Recovery = 46% Analysis Date = 02/11/17 Pct Recovery = 47% Analysis Date = 02/11/17 Pct Recovery = 47% Analysis Date = 02/10/17 Pct Recovery = 47% Analysis Date = 02/10/17 Pct Recovery = 47% Analysis Date = 02/09/17 Pct Recovery = 47% Analysis Date = 02/09/17 Pct Recovery = 47% Analysis Date = 02/08/17 Pct Recovery = 48% Analysis Date = 02/08/17 Pct Recovery = 48% Analysis Date = 02/06/17 Pct Recovery = 48% Analysis Date = 02/06/17 Pct Recovery = 48% Analysis Date = 02/05/17 Pct Recovery = 49% Analysis Date = 02/05/17 Pct Recovery = 49% Analysis Date = 02/04/17 Pct Recovery = 49% Analysis Date = 02/04/17 Pct Recovery = 49% Analysis Date = 02/03/17 Pct Recovery = 49% Analysis Date = 02/03/17 Pct Recovery = 49% Analysis Date = 02/02/17 Pct Recovery = 50% Analysis Date = 02/02/17 Pct Recovery = 50% Analysis Date = 02/01/17 Pct Recovery = 50% Analysis Date = 02/01/17 Pct Recovery = 50% Analysis Date = 01/31/17 Pct Recovery = 51% Analysis Date = 01/31/17 Pct Recovery = 51% Analysis Date = 01/30/17 Pct Recovery = 51% Analysis Date = 01/30/17 Pct Recovery = 51% Analysis Date = 01/28/17 Pct Recovery = 52% Analysis Date = 01/28/17 Pct Recovery = 52% Analysis Date = 01/27/17 Pct Recovery = 52% Analysis Date = 01/27/17 Pct Recovery = 52% Analysis Date = 01/26/17 Pct Recovery = 52% Analysis Date = 01/26/17 Pct Recovery = 52% Analysis Date = 01/25/17 Pct Recovery = 53% Analysis Date = 01/25/17 Pct Recovery = 53% Analysis Date = 01/24/17 Pct Recovery = 53% Analysis Date = 01/24/17 Pct Recovery = 53% Analysis Date = 01/23/17 Pct Recovery = 54% Analysis Date = 01/23/17 Pct Recovery = 54% Analysis Date = 01/22/17 Pct Recovery = 54% Analysis Date = 01/22/17 Pct Recovery = 54% Analysis Date = 01/21/17 Pct Recovery = 54% Analysis Date = 01/21/17 Pct Recovery = 54% Analysis Date = 01/19/17 Pct Recovery = 55% Analysis Date = 01/19/17 Pct Recovery = 55% Analysis Date = 01/18/17 Pct Recovery = 55% Analysis Date = 01/18/17 Pct Recovery = 55% Analysis Date = 01/17/17 Pct Recovery = 56% Analysis Date = 01/17/17 Pct Recovery = 56% Analysis Date = 01/16/17 Pct Recovery = 56% Analysis Date = 01/16/17 Pct Recovery = 56% Analysis Date = 01/15/17 Pct Recovery = 56% Analysis Date = 01/15/17 Pct Recovery = 56% Analysis Date = 01/14/17 Pct Recovery = 57% Analysis Date = 01/14/17 Pct Recovery = 57% Analysis Date = 01/13/17 Pct Recovery = 57% Analysis Date = 01/13/17 Pct Recovery = 57% Analysis Date = 01/12/17 Pct Recovery = 58% Analysis Date = 01/12/17 Pct Recovery = 58% Analysis Date = 01/10/17 Pct Recovery = 58% Analysis Date = 01/10/17 Pct Recovery = 58% Analysis Date = 01/09/17 Pct Recovery = 59% Analysis Date = 01/09/17 Pct Recovery = 59% Analysis Date = 01/08/17 Pct Recovery = 59% Analysis Date = 01/08/17 Pct Recovery = 59% Analysis Date = 01/07/17 Pct Recovery = 59% Analysis Date = 01/07/17 Pct Recovery = 59% Analysis Date = 01/06/17 Pct Recovery = 60% Analysis Date = 01/06/17 Pct Recovery = 60% Analysis Date = 01/05/17 Pct Recovery = 60% Analysis Date = 01/05/17 Pct Recovery = 60% Analysis Date = 01/04/17 Pct Recovery = 61% Analysis Date = 01/04/17 Pct Recovery = 61% Analysis Date = 01/03/17 Pct Recovery = 61% Analysis Date = 01/03/17 Pct Recovery = 61% Analysis Date = 01/01/17 Pct Recovery = 61% Analysis Date = 01/01/17 Pct Recovery = 61% Analysis Date = 12/31/16 Pct Recovery = 62% Analysis Date = 12/31/16 Pct Recovery = 62% Analysis Date = 12/30/16 Pct Recovery = 62% Analysis Date = 12/30/16 Pct Recovery = 62% Analysis Date = 12/29/16 Pct Recovery = 63% Analysis Date = 12/29/16 Pct Recovery = 63% Analysis Date = 12/28/16 Pct Recovery = 63% Analysis Date = 12/28/16 Pct Recovery = 63% Analysis Date = 12/27/16 Pct Recovery = 64% Analysis Date = 12/27/16 Pct Recovery = 64% Analysis Date = 12/26/16 Pct Recovery = 64% Analysis Date = 12/26/16 Pct Recovery = 64% Analysis Date = 12/25/16 Pct Recovery = 64% Analysis Date = 12/25/16 Pct Recovery = 64% Analysis Date = 12/23/16 Pct Recovery = 65% Analysis Date = 12/23/16 Pct Recovery = 65% Analysis Date = 12/22/16 Pct Recovery = 65% Analysis Date = 12/22/16 Pct Recovery = 65% Analysis Date = 12/21/16 Pct Recovery = 66% Analysis Date = 12/21/16 Pct Recovery = 66% Analysis Date = 12/20/16 Pct Recovery = 66% Analysis Date = 12/20/16 Pct Recovery = 66% Analysis Date = 12/19/16 Pct Recovery = 66% Analysis Date = 12/19/16 Pct Recovery = 66% Analysis Date = 12/18/16 Pct Recovery = 67% Analysis Date = 12/18/16 Pct Recovery = 67% Analysis Date = 12/17/16 Pct Recovery = 67% Analysis Date = 12/17/16 Pct Recovery = 67% Analysis Date = 12/16/16 Pct Recovery = 68% Analysis Date = 12/16/16 Pct Recovery = 68% Analysis Date = 12/14/16 Pct Recovery = 68% Analysis Date = 12/14/16 Pct Recovery = 68% Analysis Date = 12/13/16 Pct Recovery = 68% Analysis Date = 12/13/16 Pct Recovery = 68% Analysis Date = 12/12/16 Pct Recovery = 69% Analysis Date = 12/12/16 Pct Recovery = 69% Analysis Date = 12/11/16 Pct Recovery = 69% Analysis Date = 12/11/16 Pct Recovery = 69% Analysis Date = 12/10/16 Pct Recovery = 70% Analysis Date = 12/10/16 Pct Recovery = 70% Analysis Date = 12/09/16 Pct Recovery = 70% Analysis Date = 12/09/16 Pct Recovery = 70% Analysis Date = 12/08/16 Pct Recovery = 71% Analysis Date = 12/08/16 Pct Recovery = 71% Analysis Date = 12/07/16 Pct Recovery = 71% Analysis Date = 12/07/16 Pct Recovery = 71% Analysis Date = 12/05/16 Pct Recovery = 71% Analysis Date = 12/05/16 Pct Recovery = 71% Analysis Date = 12/04/16 Pct Recovery = 72% Analysis Date = 12/04/16 Pct Recovery = 72% Analysis Date = 12/03/16 Pct Recovery = 72% Analysis Date = 12/03/16 Pct Recovery = 72% Analysis Date = 12/02/16 Pct Recovery = 73% Analysis Date = 12/02/16 Pct Recovery = 73% Analysis Date = 12/01/16 Pct Recovery = 73% Analysis Date = 12/01/16 Pct Recovery = 73% Analysis Date = 11/30/16 Pct Recovery = 73% Analysis Date = 11/30/16 Pct Recovery = 73% Analysis Date = 11/29/16 Pct Recovery = 74% Analysis Date = 11/29/16 Pct Recovery = 74% Analysis Date = 11/28/16 Pct Recovery = 74% Analysis Date = 11/28/16 Pct Recovery = 74% Analysis Date = 11/26/16 Pct Recovery = 75% Analysis Date = 11/26/16 Pct Recovery = 75% Analysis Date = 11/25/16 Pct Recovery = 75% Analysis Date = 11/25/16 Pct Recovery = 75% Analysis Date = 11/24/16 Pct Recovery = 76% Analysis Date = 11/24/16 Pct Recovery = 76% Analysis Date = 11/23/16 Pct Recovery = 76% Analysis Date = 11/23/16 Pct Recovery = 76% Analysis Date = 11/22/16 Pct Recovery = 76% Analysis Date = 11/22/16 Pct Recovery = 76% Analysis Date = 11/21/16 Pct Recovery = 77% Analysis Date = 11/21/16 Pct Recovery = 77% Analysis Date = 11/20/16 Pct Recovery = 77% Analysis Date = 11/20/16 Pct Recovery = 77% Analysis Date = 11/19/16 Pct Recovery = 78% Analysis Date = 11/19/16 Pct Recovery = 78% Analysis Date = 11/17/16 Pct Recovery = 78% Analysis Date = 11/17/16 Pct Recovery = 78% Analysis Date = 11/16/16 Pct Recovery = 78% Analysis Date = 11/16/16 Pct Recovery = 78% Analysis Date = 11/15/16 Pct Recovery = 79% Analysis Date = 11/15/16 Pct Recovery = 79% Analysis Date = 11/14/16 Pct Recovery = 79% Analysis Date = 11/14/16 Pct Recovery = 79% Analysis Date = 11/13/16 Pct Recovery = 80% Analysis Date = 11/13/16 Pct Recovery = 80% Analysis Date = 11/12/16 Pct Recovery = 80% Analysis Date = 11/12/16 Pct Recovery = 80% Analysis Date = 11/11/16 Pct Recovery = 80% Analysis Date = 11/11/16 Pct Recovery = 80% Analysis Date = 11/10/16 Pct Recovery = 81% Analysis Date = 11/10/16 Pct Recovery = 81% Analysis Date = 11/08/16 Pct Recovery = 81% Analysis Date = 11/08/16 Pct Recovery = 81% Analysis Date = 11/07/16 Pct Recovery = 82% Analysis Date = 11/07/16 Pct Recovery = 82% Analysis Date = 11/06/16 Pct Recovery = 82% Analysis Date = 11/06/16 Pct Recovery = 82% Analysis Date = 11/05/16 Pct Recovery = 83% Analysis Date = 11/05/16 Pct Recovery = 83% Analysis Date = 11/04/16 Pct Recovery = 83% Analysis Date = 11/04/16 Pct Recovery = 83% Analysis Date = 11/03/16 Pct Recovery = 83% Analysis Date = 11/03/16 Pct Recovery = 83% Analysis Date = 11/02/16 Pct Recovery = 84% Analysis Date = 11/02/16 Pct Recovery = 84% Analysis Date = 11/01/16 Pct Recovery = 84% Analysis Date = 11/01/16 Pct Recovery = 84% Analysis Date = 10/30/16 Pct Recovery = 85% Analysis Date = 10/30/16 Pct Recovery = 85% Analysis Date = 10/29/16 Pct Recovery = 85% Analysis Date = 10/29/16 Pct Recovery = 85% Analysis Date = 10/28/16 Pct Recovery = 85% Analysis Date = 10/28/16 Pct Recovery = 85% Analysis Date = 10/27/16 Pct Recovery = 86% Analysis Date = 10/27/16 Pct Recovery = 86% Analysis Date = 10/26/16 Pct Recovery = 86% Analysis Date = 10/26/16 Pct Recovery = 86% Analysis Date = 10/25/16 Pct Recovery = 87% Analysis Date = 10/25/16 Pct Recovery = 87% Analysis Date = 10/24/16 Pct Recovery = 87% Analysis Date = 10/24/16 Pct Recovery = 87% Analysis Date = 10/23/16 Pct Recovery = 87% Analysis Date = 10/23/16 Pct Recovery = 87% Analysis Date = 10/21/16 Pct Recovery = 88% Analysis Date = 10/21/16 Pct Recovery = 88% Analysis Date = 10/20/16 Pct Recovery = 88% Analysis Date = 10/20/16 Pct Recovery = 88% Analysis Date = 10/19/16 Pct Recovery = 89% Analysis Date = 10/19/16 Pct Recovery = 89% Analysis Date = 10/18/16 Pct Recovery = 89% Analysis Date = 10/18/16 Pct Recovery = 89% Analysis Date = 10/17/16 Pct Recovery = 90% Analysis Date = 10/17/16 Pct Recovery = 90% Analysis Date = 10/16/16 Pct Recovery = 90% Analysis Date = 10/16/16 Pct Recovery = 90% Analysis Date = 10/15/16 Pct Recovery = 90% Analysis Date = 10/15/16 Pct Recovery = 90% Analysis Date = 10/14/16 Pct Recovery = 91% Analysis Date = 10/14/16 Pct Recovery = 91% Analysis Date = 10/12/16 Pct Recovery = 91% Analysis Date = 10/12/16 Pct Recovery = 91% Analysis Date = 10/11/16 Pct Recovery = 92% Analysis Date = 10/11/16 Pct Recovery = 92% Analysis Date = 10/10/16 Pct Recovery = 92% Analysis Date = 10/10/16 Pct Recovery = 92% Analysis Date = 10/09/16 Pct Recovery = 92% Analysis Date = 10/09/16 Pct Recovery = 92% Analysis Date = 10/08/16 Pct Recovery = 93% Analysis Date = 10/08/16 Pct Recovery = 93% Analysis Date = 10/07/16 Pct Recovery = 93% Analysis Date = 10/07/16 Pct Recovery = 93% Analysis Date = 10/06/16 Pct Recovery = 94% Analysis Date = 10/06/16 Pct Recovery = 94% Analysis Date = 10/05/16 Pct Recovery = 94% Analysis Date = 10/05/16 Pct Recovery = 94% Analysis Date = 10/03/16 Pct Recovery = 95% Analysis Date = 10/03/16 Pct Recovery = 95% Analysis Date = 10/02/16 Pct Recovery = 95% Analysis Date = 10/02/16 Pct Recovery = 95% Analysis Date = 10/01/16 Pct Recovery = 95% Analysis Date = 10/01/16 Pct Recovery = 95% Analysis Date = 09/30/16 Pct Recovery = 96% Analysis Date = 09/30/16 Pct Recovery = 96% Analysis Date = 09/29/16 Pct Recovery = 96% Analysis Date = 09/29/16 Pct Recovery = 96% Analysis Date = 09/28/16 Pct Recovery = 97% Analysis Date = 09/28/16 Pct Recovery = 97% Analysis Date = 09/27/16 Pct Recovery = 97% Analysis Date = 09/27/16 Pct Recovery = 97% Analysis Date = 09/26/16 Pct Recovery = 97% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
17-ALPHA-ESTRADIOL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 6 74% 30% 68% 36%
Total 6 74% 30% 68% 36%

Sample Statistics
17-ALPHA-ESTRADIOL

Characteristic N % % Basis
Plotted 6 55% Spiked
Estimated Values 3 27% Spiked
Deleted Values 2 11% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 12 .  
False Negatives 5 45% 5 out of 11
Not Spiked 7 .  
False Positives 0 0% 0 out of 6

BQS OBSP Determination:
17-ALPHA-ETHYNYLESTRADIOL
METHOD: 6434 , TESTIDCODE: 63207GM006
Open Data Set

Analysis Date = 05/24/17 SpikeMix = ERA 04121615: 0 µl Pct Recovery = 95% Analysis Date = 04/19/17 SpikeMix = ERA 04121615: 0 µl & ERA 04121614: 0 µl Pct Recovery = 52% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
17-ALPHA-ETHYNYLESTRADIOL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 2 74% 31% 74% 32%
Total 2 74% 31% 74% 32%

Sample Statistics
17-ALPHA-ETHYNYLESTRADIOL

Characteristic N % % Basis
Plotted 2 18% Spiked
Estimated Values 0 0% Spiked
Deleted Values 1 5% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 12 .  
False Negatives 9 82% 9 out of 11
Not Spiked 7 .  
False Positives 0 0% 0 out of 7

BQS OBSP Determination:
17-BETA-ESTRADIOL
METHOD: 6434 , TESTIDCODE: 63164GM006
Open Data Set

Analysis Date = 09/26/16 SpikeMix = Abs 051616sed4H3: 0 µl & Abs 051616sed4H2: 0 µl Pct Recovery = 120% Analysis Date = 09/26/16 SpikeMix = Abs 051616sed4H3: 0 µl & Abs 051616sed4H1: 0 µl Pct Recovery = 81% Analysis Date = 09/26/16 SpikeMix = Abs 051616sed4H2: 0 µl & Abs 051616sed4L3: 0 µl Pct Recovery = 60% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
17-BETA-ESTRADIOL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 3 87% 30% 81% 44%
Total 3 87% 30% 81% 44%

Sample Statistics
17-BETA-ESTRADIOL

Characteristic N % % Basis
Plotted 3 27% Spiked
Estimated Values 1 9% Spiked
Deleted Values 2 11% Spiked + Not Spiked
Spiked, Censored 1 9% Spiked
Spiked 12 .  
False Negatives 7 64% 7 out of 11
Not Spiked 7 .  
False Positives 0 0% 0 out of 6

BQS OBSP Determination:
3-BETA-COPROSTANOL
METHOD: 6434 , TESTIDCODE: 63170GM006
Open Data Set

Analysis Date = 09/26/16 SpikeMix = Abs 051616sed4H3: 0 µl & Abs 051616sed4H2: 0 µl Pct Recovery = 36% Analysis Date = 09/26/16 SpikeMix = Abs 051616sed4H1: 0 µl & Abs 051616sed4H2: 0 µl Pct Recovery = 36% Analysis Date = 09/26/16 SpikeMix = Abs 051616sed4H2: 0 µl & Abs 051616sed4L3: 0 µl Pct Recovery = 35% Analysis Date = 09/26/16 SpikeMix = Abs 051616sed4H1: 0 µl & Abs 051616sed4L2: 0 µl Pct Recovery = 89% Analysis Date = 05/24/17 SpikeMix = ERA 04121614: 0 µl & Abs 051616sed4L: 0 µl Pct Recovery = 55% Analysis Date = 05/09/17 SpikeMix = ERA 04121614: 0 µl & Abs 051616sed4L3: 0 µl Pct Recovery = 54% Analysis Date = 04/19/17 SpikeMix = ERA 04121613: 0 µl & ERA 04121614: 0 µl Pct Recovery = 50% Analysis Date = 03/17/17 SpikeMix = ERA 04121613: 0 µl & ERA 04121614: 0 µl Pct Recovery = 57% Analysis Date = 03/17/17 SpikeMix = ERA 04121614: 0 µl & ERA 04121615: 0 µl Pct Recovery = 56% Analysis Date = 05/24/17 Pct Recovery = 55% Analysis Date = 05/22/17 Pct Recovery = 55% Analysis Date = 05/22/17 Pct Recovery = 55% Analysis Date = 05/21/17 Pct Recovery = 55% Analysis Date = 05/21/17 Pct Recovery = 55% Analysis Date = 05/20/17 Pct Recovery = 55% Analysis Date = 05/20/17 Pct Recovery = 55% Analysis Date = 05/19/17 Pct Recovery = 55% Analysis Date = 05/19/17 Pct Recovery = 55% Analysis Date = 05/18/17 Pct Recovery = 55% Analysis Date = 05/18/17 Pct Recovery = 55% Analysis Date = 05/16/17 Pct Recovery = 54% Analysis Date = 05/16/17 Pct Recovery = 54% Analysis Date = 05/15/17 Pct Recovery = 54% Analysis Date = 05/15/17 Pct Recovery = 54% Analysis Date = 05/14/17 Pct Recovery = 54% Analysis Date = 05/14/17 Pct Recovery = 54% Analysis Date = 05/13/17 Pct Recovery = 54% Analysis Date = 05/13/17 Pct Recovery = 54% Analysis Date = 05/12/17 Pct Recovery = 54% Analysis Date = 05/12/17 Pct Recovery = 54% Analysis Date = 05/10/17 Pct Recovery = 54% Analysis Date = 05/10/17 Pct Recovery = 54% Analysis Date = 05/09/17 Pct Recovery = 53% Analysis Date = 05/09/17 Pct Recovery = 53% Analysis Date = 05/08/17 Pct Recovery = 53% Analysis Date = 05/08/17 Pct Recovery = 53% Analysis Date = 05/07/17 Pct Recovery = 53% Analysis Date = 05/07/17 Pct Recovery = 53% Analysis Date = 05/06/17 Pct Recovery = 53% Analysis Date = 05/06/17 Pct Recovery = 53% Analysis Date = 05/04/17 Pct Recovery = 53% Analysis Date = 05/04/17 Pct Recovery = 53% Analysis Date = 05/03/17 Pct Recovery = 53% Analysis Date = 05/03/17 Pct Recovery = 53% Analysis Date = 05/02/17 Pct Recovery = 52% Analysis Date = 05/02/17 Pct Recovery = 52% Analysis Date = 05/01/17 Pct Recovery = 52% Analysis Date = 05/01/17 Pct Recovery = 52% Analysis Date = 04/30/17 Pct Recovery = 52% Analysis Date = 04/30/17 Pct Recovery = 52% Analysis Date = 04/28/17 Pct Recovery = 52% Analysis Date = 04/28/17 Pct Recovery = 52% Analysis Date = 04/27/17 Pct Recovery = 52% Analysis Date = 04/27/17 Pct Recovery = 52% Analysis Date = 04/26/17 Pct Recovery = 52% Analysis Date = 04/26/17 Pct Recovery = 52% Analysis Date = 04/25/17 Pct Recovery = 51% Analysis Date = 04/25/17 Pct Recovery = 51% Analysis Date = 04/24/17 Pct Recovery = 51% Analysis Date = 04/24/17 Pct Recovery = 51% Analysis Date = 04/22/17 Pct Recovery = 51% Analysis Date = 04/22/17 Pct Recovery = 51% Analysis Date = 04/21/17 Pct Recovery = 51% Analysis Date = 04/21/17 Pct Recovery = 51% Analysis Date = 04/20/17 Pct Recovery = 51% Analysis Date = 04/20/17 Pct Recovery = 51% Analysis Date = 04/19/17 Pct Recovery = 51% Analysis Date = 04/19/17 Pct Recovery = 51% Analysis Date = 04/18/17 Pct Recovery = 51% Analysis Date = 04/18/17 Pct Recovery = 51% Analysis Date = 04/16/17 Pct Recovery = 51% Analysis Date = 04/16/17 Pct Recovery = 51% Analysis Date = 04/15/17 Pct Recovery = 51% Analysis Date = 04/15/17 Pct Recovery = 51% Analysis Date = 04/14/17 Pct Recovery = 51% Analysis Date = 04/14/17 Pct Recovery = 51% Analysis Date = 04/13/17 Pct Recovery = 52% Analysis Date = 04/13/17 Pct Recovery = 52% Analysis Date = 04/12/17 Pct Recovery = 52% Analysis Date = 04/12/17 Pct Recovery = 52% Analysis Date = 04/10/17 Pct Recovery = 52% Analysis Date = 04/10/17 Pct Recovery = 52% Analysis Date = 04/09/17 Pct Recovery = 52% Analysis Date = 04/09/17 Pct Recovery = 52% Analysis Date = 04/08/17 Pct Recovery = 52% Analysis Date = 04/08/17 Pct Recovery = 52% Analysis Date = 04/07/17 Pct Recovery = 53% Analysis Date = 04/07/17 Pct Recovery = 53% Analysis Date = 04/06/17 Pct Recovery = 53% Analysis Date = 04/06/17 Pct Recovery = 53% Analysis Date = 04/04/17 Pct Recovery = 53% Analysis Date = 04/04/17 Pct Recovery = 53% Analysis Date = 04/03/17 Pct Recovery = 53% Analysis Date = 04/03/17 Pct Recovery = 53% Analysis Date = 04/02/17 Pct Recovery = 53% Analysis Date = 04/02/17 Pct Recovery = 53% Analysis Date = 04/01/17 Pct Recovery = 54% Analysis Date = 04/01/17 Pct Recovery = 54% Analysis Date = 03/31/17 Pct Recovery = 54% Analysis Date = 03/31/17 Pct Recovery = 54% Analysis Date = 03/29/17 Pct Recovery = 54% Analysis Date = 03/29/17 Pct Recovery = 54% Analysis Date = 03/28/17 Pct Recovery = 54% Analysis Date = 03/28/17 Pct Recovery = 54% Analysis Date = 03/27/17 Pct Recovery = 54% Analysis Date = 03/27/17 Pct Recovery = 54% Analysis Date = 03/26/17 Pct Recovery = 55% Analysis Date = 03/26/17 Pct Recovery = 55% Analysis Date = 03/25/17 Pct Recovery = 55% Analysis Date = 03/25/17 Pct Recovery = 55% Analysis Date = 03/23/17 Pct Recovery = 55% Analysis Date = 03/23/17 Pct Recovery = 55% Analysis Date = 03/22/17 Pct Recovery = 55% Analysis Date = 03/22/17 Pct Recovery = 55% Analysis Date = 03/21/17 Pct Recovery = 55% Analysis Date = 03/21/17 Pct Recovery = 55% Analysis Date = 03/20/17 Pct Recovery = 56% Analysis Date = 03/20/17 Pct Recovery = 56% Analysis Date = 03/19/17 Pct Recovery = 56% Analysis Date = 03/19/17 Pct Recovery = 56% Analysis Date = 03/17/17 Pct Recovery = 56% Analysis Date = 03/17/17 Pct Recovery = 56% Analysis Date = 03/16/17 Pct Recovery = 56% Analysis Date = 03/16/17 Pct Recovery = 56% Analysis Date = 03/15/17 Pct Recovery = 56% Analysis Date = 03/15/17 Pct Recovery = 56% Analysis Date = 03/14/17 Pct Recovery = 56% Analysis Date = 03/14/17 Pct Recovery = 56% Analysis Date = 03/13/17 Pct Recovery = 56% Analysis Date = 03/13/17 Pct Recovery = 56% Analysis Date = 03/11/17 Pct Recovery = 56% Analysis Date = 03/11/17 Pct Recovery = 56% Analysis Date = 03/10/17 Pct Recovery = 56% Analysis Date = 03/10/17 Pct Recovery = 56% Analysis Date = 03/09/17 Pct Recovery = 56% Analysis Date = 03/09/17 Pct Recovery = 56% Analysis Date = 03/08/17 Pct Recovery = 56% Analysis Date = 03/08/17 Pct Recovery = 56% Analysis Date = 03/07/17 Pct Recovery = 56% Analysis Date = 03/07/17 Pct Recovery = 56% Analysis Date = 03/05/17 Pct Recovery = 56% Analysis Date = 03/05/17 Pct Recovery = 56% Analysis Date = 03/04/17 Pct Recovery = 56% Analysis Date = 03/04/17 Pct Recovery = 56% Analysis Date = 03/03/17 Pct Recovery = 56% Analysis Date = 03/03/17 Pct Recovery = 56% Analysis Date = 03/02/17 Pct Recovery = 56% Analysis Date = 03/02/17 Pct Recovery = 56% Analysis Date = 03/01/17 Pct Recovery = 56% Analysis Date = 03/01/17 Pct Recovery = 56% Analysis Date = 02/27/17 Pct Recovery = 55% Analysis Date = 02/27/17 Pct Recovery = 55% Analysis Date = 02/26/17 Pct Recovery = 55% Analysis Date = 02/26/17 Pct Recovery = 55% Analysis Date = 02/25/17 Pct Recovery = 55% Analysis Date = 02/25/17 Pct Recovery = 55% Analysis Date = 02/24/17 Pct Recovery = 55% Analysis Date = 02/24/17 Pct Recovery = 55% Analysis Date = 02/23/17 Pct Recovery = 55% Analysis Date = 02/23/17 Pct Recovery = 55% Analysis Date = 02/21/17 Pct Recovery = 55% Analysis Date = 02/21/17 Pct Recovery = 55% Analysis Date = 02/20/17 Pct Recovery = 55% Analysis Date = 02/20/17 Pct Recovery = 55% Analysis Date = 02/19/17 Pct Recovery = 55% Analysis Date = 02/19/17 Pct Recovery = 55% Analysis Date = 02/18/17 Pct Recovery = 55% Analysis Date = 02/18/17 Pct Recovery = 55% Analysis Date = 02/17/17 Pct Recovery = 55% Analysis Date = 02/17/17 Pct Recovery = 55% Analysis Date = 02/15/17 Pct Recovery = 55% Analysis Date = 02/15/17 Pct Recovery = 55% Analysis Date = 02/14/17 Pct Recovery = 55% Analysis Date = 02/14/17 Pct Recovery = 55% Analysis Date = 02/13/17 Pct Recovery = 55% Analysis Date = 02/13/17 Pct Recovery = 55% Analysis Date = 02/12/17 Pct Recovery = 55% Analysis Date = 02/12/17 Pct Recovery = 55% Analysis Date = 02/11/17 Pct Recovery = 55% Analysis Date = 02/11/17 Pct Recovery = 55% Analysis Date = 02/09/17 Pct Recovery = 55% Analysis Date = 02/09/17 Pct Recovery = 55% Analysis Date = 02/08/17 Pct Recovery = 55% Analysis Date = 02/08/17 Pct Recovery = 55% Analysis Date = 02/07/17 Pct Recovery = 55% Analysis Date = 02/07/17 Pct Recovery = 55% Analysis Date = 02/06/17 Pct Recovery = 55% Analysis Date = 02/06/17 Pct Recovery = 55% Analysis Date = 02/05/17 Pct Recovery = 55% Analysis Date = 02/05/17 Pct Recovery = 55% Analysis Date = 02/03/17 Pct Recovery = 54% Analysis Date = 02/03/17 Pct Recovery = 54% Analysis Date = 02/02/17 Pct Recovery = 54% Analysis Date = 02/02/17 Pct Recovery = 54% Analysis Date = 02/01/17 Pct Recovery = 54% Analysis Date = 02/01/17 Pct Recovery = 54% Analysis Date = 01/31/17 Pct Recovery = 54% Analysis Date = 01/31/17 Pct Recovery = 54% Analysis Date = 01/30/17 Pct Recovery = 54% Analysis Date = 01/30/17 Pct Recovery = 54% Analysis Date = 01/28/17 Pct Recovery = 54% Analysis Date = 01/28/17 Pct Recovery = 54% Analysis Date = 01/27/17 Pct Recovery = 54% Analysis Date = 01/27/17 Pct Recovery = 54% Analysis Date = 01/26/17 Pct Recovery = 54% Analysis Date = 01/26/17 Pct Recovery = 54% Analysis Date = 01/25/17 Pct Recovery = 54% Analysis Date = 01/25/17 Pct Recovery = 54% Analysis Date = 01/24/17 Pct Recovery = 54% Analysis Date = 01/24/17 Pct Recovery = 54% Analysis Date = 01/22/17 Pct Recovery = 54% Analysis Date = 01/22/17 Pct Recovery = 54% Analysis Date = 01/21/17 Pct Recovery = 54% Analysis Date = 01/21/17 Pct Recovery = 54% Analysis Date = 01/20/17 Pct Recovery = 54% Analysis Date = 01/20/17 Pct Recovery = 54% Analysis Date = 01/19/17 Pct Recovery = 54% Analysis Date = 01/19/17 Pct Recovery = 54% Analysis Date = 01/18/17 Pct Recovery = 54% Analysis Date = 01/18/17 Pct Recovery = 54% Analysis Date = 01/16/17 Pct Recovery = 54% Analysis Date = 01/16/17 Pct Recovery = 54% Analysis Date = 01/15/17 Pct Recovery = 54% Analysis Date = 01/15/17 Pct Recovery = 54% Analysis Date = 01/14/17 Pct Recovery = 54% Analysis Date = 01/14/17 Pct Recovery = 54% Analysis Date = 01/13/17 Pct Recovery = 54% Analysis Date = 01/13/17 Pct Recovery = 54% Analysis Date = 01/12/17 Pct Recovery = 54% Analysis Date = 01/12/17 Pct Recovery = 54% Analysis Date = 01/10/17 Pct Recovery = 54% Analysis Date = 01/10/17 Pct Recovery = 54% Analysis Date = 01/09/17 Pct Recovery = 53% Analysis Date = 01/09/17 Pct Recovery = 53% Analysis Date = 01/08/17 Pct Recovery = 53% Analysis Date = 01/08/17 Pct Recovery = 53% Analysis Date = 01/07/17 Pct Recovery = 53% Analysis Date = 01/07/17 Pct Recovery = 53% Analysis Date = 01/06/17 Pct Recovery = 53% Analysis Date = 01/06/17 Pct Recovery = 53% Analysis Date = 01/04/17 Pct Recovery = 53% Analysis Date = 01/04/17 Pct Recovery = 53% Analysis Date = 01/03/17 Pct Recovery = 53% Analysis Date = 01/03/17 Pct Recovery = 53% Analysis Date = 01/02/17 Pct Recovery = 53% Analysis Date = 01/02/17 Pct Recovery = 53% Analysis Date = 01/01/17 Pct Recovery = 53% Analysis Date = 01/01/17 Pct Recovery = 53% Analysis Date = 12/31/16 Pct Recovery = 53% Analysis Date = 12/31/16 Pct Recovery = 53% Analysis Date = 12/29/16 Pct Recovery = 53% Analysis Date = 12/29/16 Pct Recovery = 53% Analysis Date = 12/28/16 Pct Recovery = 53% Analysis Date = 12/28/16 Pct Recovery = 53% Analysis Date = 12/27/16 Pct Recovery = 53% Analysis Date = 12/27/16 Pct Recovery = 53% Analysis Date = 12/26/16 Pct Recovery = 53% Analysis Date = 12/26/16 Pct Recovery = 53% Analysis Date = 12/25/16 Pct Recovery = 53% Analysis Date = 12/25/16 Pct Recovery = 53% Analysis Date = 12/23/16 Pct Recovery = 53% Analysis Date = 12/23/16 Pct Recovery = 53% Analysis Date = 12/22/16 Pct Recovery = 53% Analysis Date = 12/22/16 Pct Recovery = 53% Analysis Date = 12/21/16 Pct Recovery = 53% Analysis Date = 12/21/16 Pct Recovery = 53% Analysis Date = 12/20/16 Pct Recovery = 53% Analysis Date = 12/20/16 Pct Recovery = 53% Analysis Date = 12/19/16 Pct Recovery = 53% Analysis Date = 12/19/16 Pct Recovery = 53% Analysis Date = 12/17/16 Pct Recovery = 53% Analysis Date = 12/17/16 Pct Recovery = 53% Analysis Date = 12/16/16 Pct Recovery = 52% Analysis Date = 12/16/16 Pct Recovery = 52% Analysis Date = 12/15/16 Pct Recovery = 52% Analysis Date = 12/15/16 Pct Recovery = 52% Analysis Date = 12/14/16 Pct Recovery = 52% Analysis Date = 12/14/16 Pct Recovery = 52% Analysis Date = 12/13/16 Pct Recovery = 52% Analysis Date = 12/13/16 Pct Recovery = 52% Analysis Date = 12/11/16 Pct Recovery = 52% Analysis Date = 12/11/16 Pct Recovery = 52% Analysis Date = 12/10/16 Pct Recovery = 52% Analysis Date = 12/10/16 Pct Recovery = 52% Analysis Date = 12/09/16 Pct Recovery = 52% Analysis Date = 12/09/16 Pct Recovery = 52% Analysis Date = 12/08/16 Pct Recovery = 52% Analysis Date = 12/08/16 Pct Recovery = 52% Analysis Date = 12/07/16 Pct Recovery = 52% Analysis Date = 12/07/16 Pct Recovery = 52% Analysis Date = 12/05/16 Pct Recovery = 52% Analysis Date = 12/05/16 Pct Recovery = 52% Analysis Date = 12/04/16 Pct Recovery = 52% Analysis Date = 12/04/16 Pct Recovery = 52% Analysis Date = 12/03/16 Pct Recovery = 52% Analysis Date = 12/03/16 Pct Recovery = 52% Analysis Date = 12/02/16 Pct Recovery = 52% Analysis Date = 12/02/16 Pct Recovery = 52% Analysis Date = 12/01/16 Pct Recovery = 52% Analysis Date = 12/01/16 Pct Recovery = 52% Analysis Date = 11/29/16 Pct Recovery = 52% Analysis Date = 11/29/16 Pct Recovery = 52% Analysis Date = 11/28/16 Pct Recovery = 52% Analysis Date = 11/28/16 Pct Recovery = 52% Analysis Date = 11/27/16 Pct Recovery = 52% Analysis Date = 11/27/16 Pct Recovery = 52% Analysis Date = 11/26/16 Pct Recovery = 52% Analysis Date = 11/26/16 Pct Recovery = 52% Analysis Date = 11/25/16 Pct Recovery = 52% Analysis Date = 11/25/16 Pct Recovery = 52% Analysis Date = 11/23/16 Pct Recovery = 52% Analysis Date = 11/23/16 Pct Recovery = 52% Analysis Date = 11/22/16 Pct Recovery = 51% Analysis Date = 11/22/16 Pct Recovery = 51% Analysis Date = 11/21/16 Pct Recovery = 51% Analysis Date = 11/21/16 Pct Recovery = 51% Analysis Date = 11/20/16 Pct Recovery = 51% Analysis Date = 11/20/16 Pct Recovery = 51% Analysis Date = 11/19/16 Pct Recovery = 51% Analysis Date = 11/19/16 Pct Recovery = 51% Analysis Date = 11/17/16 Pct Recovery = 51% Analysis Date = 11/17/16 Pct Recovery = 51% Analysis Date = 11/16/16 Pct Recovery = 51% Analysis Date = 11/16/16 Pct Recovery = 51% Analysis Date = 11/15/16 Pct Recovery = 51% Analysis Date = 11/15/16 Pct Recovery = 51% Analysis Date = 11/14/16 Pct Recovery = 51% Analysis Date = 11/14/16 Pct Recovery = 51% Analysis Date = 11/13/16 Pct Recovery = 51% Analysis Date = 11/13/16 Pct Recovery = 51% Analysis Date = 11/11/16 Pct Recovery = 51% Analysis Date = 11/11/16 Pct Recovery = 51% Analysis Date = 11/10/16 Pct Recovery = 51% Analysis Date = 11/10/16 Pct Recovery = 51% Analysis Date = 11/09/16 Pct Recovery = 51% Analysis Date = 11/09/16 Pct Recovery = 51% Analysis Date = 11/08/16 Pct Recovery = 51% Analysis Date = 11/08/16 Pct Recovery = 51% Analysis Date = 11/07/16 Pct Recovery = 51% Analysis Date = 11/07/16 Pct Recovery = 51% Analysis Date = 11/05/16 Pct Recovery = 51% Analysis Date = 11/05/16 Pct Recovery = 51% Analysis Date = 11/04/16 Pct Recovery = 51% Analysis Date = 11/04/16 Pct Recovery = 51% Analysis Date = 11/03/16 Pct Recovery = 51% Analysis Date = 11/03/16 Pct Recovery = 51% Analysis Date = 11/02/16 Pct Recovery = 51% Analysis Date = 11/02/16 Pct Recovery = 51% Analysis Date = 11/01/16 Pct Recovery = 51% Analysis Date = 11/01/16 Pct Recovery = 51% Analysis Date = 10/30/16 Pct Recovery = 51% Analysis Date = 10/30/16 Pct Recovery = 51% Analysis Date = 10/29/16 Pct Recovery = 50% Analysis Date = 10/29/16 Pct Recovery = 50% Analysis Date = 10/28/16 Pct Recovery = 50% Analysis Date = 10/28/16 Pct Recovery = 50% Analysis Date = 10/27/16 Pct Recovery = 50% Analysis Date = 10/27/16 Pct Recovery = 50% Analysis Date = 10/26/16 Pct Recovery = 50% Analysis Date = 10/26/16 Pct Recovery = 50% Analysis Date = 10/24/16 Pct Recovery = 50% Analysis Date = 10/24/16 Pct Recovery = 50% Analysis Date = 10/23/16 Pct Recovery = 50% Analysis Date = 10/23/16 Pct Recovery = 50% Analysis Date = 10/22/16 Pct Recovery = 50% Analysis Date = 10/22/16 Pct Recovery = 50% Analysis Date = 10/21/16 Pct Recovery = 50% Analysis Date = 10/21/16 Pct Recovery = 50% Analysis Date = 10/20/16 Pct Recovery = 50% Analysis Date = 10/20/16 Pct Recovery = 50% Analysis Date = 10/18/16 Pct Recovery = 50% Analysis Date = 10/18/16 Pct Recovery = 50% Analysis Date = 10/17/16 Pct Recovery = 50% Analysis Date = 10/17/16 Pct Recovery = 50% Analysis Date = 10/16/16 Pct Recovery = 50% Analysis Date = 10/16/16 Pct Recovery = 50% Analysis Date = 10/15/16 Pct Recovery = 50% Analysis Date = 10/15/16 Pct Recovery = 50% Analysis Date = 10/14/16 Pct Recovery = 50% Analysis Date = 10/14/16 Pct Recovery = 50% Analysis Date = 10/12/16 Pct Recovery = 50% Analysis Date = 10/12/16 Pct Recovery = 50% Analysis Date = 10/11/16 Pct Recovery = 50% Analysis Date = 10/11/16 Pct Recovery = 50% Analysis Date = 10/10/16 Pct Recovery = 50% Analysis Date = 10/10/16 Pct Recovery = 50% Analysis Date = 10/09/16 Pct Recovery = 50% Analysis Date = 10/09/16 Pct Recovery = 50% Analysis Date = 10/08/16 Pct Recovery = 50% Analysis Date = 10/08/16 Pct Recovery = 50% Analysis Date = 10/06/16 Pct Recovery = 50% Analysis Date = 10/06/16 Pct Recovery = 50% Analysis Date = 10/05/16 Pct Recovery = 49% Analysis Date = 10/05/16 Pct Recovery = 49% Analysis Date = 10/04/16 Pct Recovery = 49% Analysis Date = 10/04/16 Pct Recovery = 49% Analysis Date = 10/03/16 Pct Recovery = 49% Analysis Date = 10/03/16 Pct Recovery = 49% Analysis Date = 10/02/16 Pct Recovery = 49% Analysis Date = 10/02/16 Pct Recovery = 49% Analysis Date = 09/30/16 Pct Recovery = 49% Analysis Date = 09/30/16 Pct Recovery = 49% Analysis Date = 09/29/16 Pct Recovery = 49% Analysis Date = 09/29/16 Pct Recovery = 49% Analysis Date = 09/28/16 Pct Recovery = 49% Analysis Date = 09/28/16 Pct Recovery = 49% Analysis Date = 09/27/16 Pct Recovery = 49% Analysis Date = 09/27/16 Pct Recovery = 49% Analysis Date = 09/26/16 Pct Recovery = 49% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
3-BETA-COPROSTANOL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 9 52% 16% 54% 15%
Total 9 52% 16% 54% 15%

Sample Statistics
3-BETA-COPROSTANOL

Characteristic N % % Basis
Plotted 9 82% Spiked
Estimated Values 4 36% Spiked
Deleted Values 1 5% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 12 .  
False Negatives 2 18% 2 out of 11
Not Spiked 7 .  
False Positives 0 0% 0 out of 7

BQS OBSP Determination:
4-ANDROSTENE-3,17-DIONE
METHOD: 6434 , TESTIDCODE: 64473GM006
Open Data Set

Analysis Date = 10/20/16 SpikeMix = Abs 051616sed4H3: 0 µl & Abs 051616sed4L: 0 µl Pct Recovery = 159% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
4-ANDROSTENE-3,17-DIONE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 1 159% . 159% 0%
Total 1 159% . 159% 0%

Sample Statistics
4-ANDROSTENE-3,17-DIONE

Characteristic N % % Basis
Plotted 1 20% Spiked
Estimated Values 1 20% Spiked
Deleted Values 1 5% Spiked + Not Spiked
Spiked, Censored 3 60% Spiked
Spiked 6 .  
False Negatives 1 20% 1 out of 5
Not Spiked 13 .  
False Positives 1 8% 1 out of 13

BQS OBSP Determination:
BISPHENOL A
METHOD: 6434 , TESTIDCODE: 63188GM006
Open Data Set

Analysis Date = 09/26/16 SpikeMix = Abs 051616sed4H1: 0 µl & Abs 051616sed4L2: 0 µl Pct Recovery = 307% Analysis Date = 09/26/16 SpikeMix = Abs 051616sed4H3: 0 µl & Abs 051616sed4H2: 0 µl Pct Recovery = 102% Analysis Date = 09/26/16 SpikeMix = Abs 051616sed4H1: 0 µl & Abs 051616sed4H2: 0 µl Pct Recovery = 105% Analysis Date = 09/26/16 SpikeMix = Abs 051616sed4H2: 0 µl & Abs 051616sed4L3: 0 µl Pct Recovery = 97% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
BISPHENOL A

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 4 153% 103% 103% 79%
Total 4 153% 103% 103% 79%

Sample Statistics
BISPHENOL A

Characteristic N % % Basis
Plotted 4 36% Spiked
Estimated Values 4 36% Spiked
Deleted Values 1 5% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 12 .  
False Negatives 7 64% 7 out of 11
Not Spiked 7 .  
False Positives 0 0% 0 out of 7

BQS OBSP Determination:
CHOLESTEROL
METHOD: 6434 , TESTIDCODE: 63196GM006
Open Data Set

Analysis Date = 09/26/16 SpikeMix = Abs 051616sed4H1: 0 µl & Abs 051616sed4L2: 0 µl Pct Recovery = 110% Analysis Date = 09/26/16 SpikeMix = Abs 051616sed4H3: 0 µl & Abs 051616sed4H1: 0 µl Pct Recovery = 97% Analysis Date = 09/26/16 SpikeMix = Abs 051616sed4H1: 0 µl & Abs 051616sed4H2: 0 µl Pct Recovery = 124% Analysis Date = 05/09/17 SpikeMix = ERA 04121615: 0 µl & Abs 051616sed4L: 0 µl Pct Recovery = 116% Analysis Date = 10/20/16 SpikeMix = Abs 051616sed4H3: 0 µl & Abs 051616sed4L: 0 µl Pct Recovery = 122% Analysis Date = 05/09/17 Pct Recovery = 116% Analysis Date = 05/07/17 Pct Recovery = 116% Analysis Date = 05/07/17 Pct Recovery = 116% Analysis Date = 05/06/17 Pct Recovery = 116% Analysis Date = 05/06/17 Pct Recovery = 116% Analysis Date = 05/05/17 Pct Recovery = 116% Analysis Date = 05/05/17 Pct Recovery = 116% Analysis Date = 05/04/17 Pct Recovery = 116% Analysis Date = 05/04/17 Pct Recovery = 116% Analysis Date = 05/03/17 Pct Recovery = 116% Analysis Date = 05/03/17 Pct Recovery = 116% Analysis Date = 05/02/17 Pct Recovery = 116% Analysis Date = 05/02/17 Pct Recovery = 116% Analysis Date = 05/01/17 Pct Recovery = 116% Analysis Date = 05/01/17 Pct Recovery = 116% Analysis Date = 04/30/17 Pct Recovery = 116% Analysis Date = 04/30/17 Pct Recovery = 116% Analysis Date = 04/28/17 Pct Recovery = 116% Analysis Date = 04/28/17 Pct Recovery = 116% Analysis Date = 04/27/17 Pct Recovery = 116% Analysis Date = 04/27/17 Pct Recovery = 116% Analysis Date = 04/26/17 Pct Recovery = 116% Analysis Date = 04/26/17 Pct Recovery = 116% Analysis Date = 04/25/17 Pct Recovery = 116% Analysis Date = 04/25/17 Pct Recovery = 116% Analysis Date = 04/24/17 Pct Recovery = 116% Analysis Date = 04/24/17 Pct Recovery = 116% Analysis Date = 04/23/17 Pct Recovery = 116% Analysis Date = 04/23/17 Pct Recovery = 116% Analysis Date = 04/22/17 Pct Recovery = 116% Analysis Date = 04/22/17 Pct Recovery = 116% Analysis Date = 04/21/17 Pct Recovery = 116% Analysis Date = 04/21/17 Pct Recovery = 116% Analysis Date = 04/19/17 Pct Recovery = 116% Analysis Date = 04/19/17 Pct Recovery = 116% Analysis Date = 04/18/17 Pct Recovery = 116% Analysis Date = 04/18/17 Pct Recovery = 116% Analysis Date = 04/17/17 Pct Recovery = 116% Analysis Date = 04/17/17 Pct Recovery = 116% Analysis Date = 04/16/17 Pct Recovery = 116% Analysis Date = 04/16/17 Pct Recovery = 116% Analysis Date = 04/15/17 Pct Recovery = 116% Analysis Date = 04/15/17 Pct Recovery = 116% Analysis Date = 04/14/17 Pct Recovery = 116% Analysis Date = 04/14/17 Pct Recovery = 116% Analysis Date = 04/13/17 Pct Recovery = 116% Analysis Date = 04/13/17 Pct Recovery = 116% Analysis Date = 04/12/17 Pct Recovery = 116% Analysis Date = 04/12/17 Pct Recovery = 116% Analysis Date = 04/10/17 Pct Recovery = 116% Analysis Date = 04/10/17 Pct Recovery = 116% Analysis Date = 04/09/17 Pct Recovery = 117% Analysis Date = 04/09/17 Pct Recovery = 117% Analysis Date = 04/08/17 Pct Recovery = 117% Analysis Date = 04/08/17 Pct Recovery = 117% Analysis Date = 04/07/17 Pct Recovery = 117% Analysis Date = 04/07/17 Pct Recovery = 117% Analysis Date = 04/06/17 Pct Recovery = 117% Analysis Date = 04/06/17 Pct Recovery = 117% Analysis Date = 04/05/17 Pct Recovery = 117% Analysis Date = 04/05/17 Pct Recovery = 117% Analysis Date = 04/04/17 Pct Recovery = 117% Analysis Date = 04/04/17 Pct Recovery = 117% Analysis Date = 04/03/17 Pct Recovery = 117% Analysis Date = 04/03/17 Pct Recovery = 117% Analysis Date = 04/01/17 Pct Recovery = 117% Analysis Date = 04/01/17 Pct Recovery = 117% Analysis Date = 03/31/17 Pct Recovery = 117% Analysis Date = 03/31/17 Pct Recovery = 117% Analysis Date = 03/30/17 Pct Recovery = 117% Analysis Date = 03/30/17 Pct Recovery = 117% Analysis Date = 03/29/17 Pct Recovery = 117% Analysis Date = 03/29/17 Pct Recovery = 117% Analysis Date = 03/28/17 Pct Recovery = 117% Analysis Date = 03/28/17 Pct Recovery = 117% Analysis Date = 03/27/17 Pct Recovery = 117% Analysis Date = 03/27/17 Pct Recovery = 117% Analysis Date = 03/26/17 Pct Recovery = 117% Analysis Date = 03/26/17 Pct Recovery = 117% Analysis Date = 03/25/17 Pct Recovery = 117% Analysis Date = 03/25/17 Pct Recovery = 117% Analysis Date = 03/23/17 Pct Recovery = 117% Analysis Date = 03/23/17 Pct Recovery = 117% Analysis Date = 03/22/17 Pct Recovery = 117% Analysis Date = 03/22/17 Pct Recovery = 117% Analysis Date = 03/21/17 Pct Recovery = 117% Analysis Date = 03/21/17 Pct Recovery = 117% Analysis Date = 03/20/17 Pct Recovery = 117% Analysis Date = 03/20/17 Pct Recovery = 117% Analysis Date = 03/19/17 Pct Recovery = 117% Analysis Date = 03/19/17 Pct Recovery = 117% Analysis Date = 03/18/17 Pct Recovery = 117% Analysis Date = 03/18/17 Pct Recovery = 117% Analysis Date = 03/17/17 Pct Recovery = 117% Analysis Date = 03/17/17 Pct Recovery = 117% Analysis Date = 03/16/17 Pct Recovery = 117% Analysis Date = 03/16/17 Pct Recovery = 117% Analysis Date = 03/14/17 Pct Recovery = 117% Analysis Date = 03/14/17 Pct Recovery = 117% Analysis Date = 03/13/17 Pct Recovery = 117% Analysis Date = 03/13/17 Pct Recovery = 117% Analysis Date = 03/12/17 Pct Recovery = 117% Analysis Date = 03/12/17 Pct Recovery = 117% Analysis Date = 03/11/17 Pct Recovery = 117% Analysis Date = 03/11/17 Pct Recovery = 117% Analysis Date = 03/10/17 Pct Recovery = 117% Analysis Date = 03/10/17 Pct Recovery = 117% Analysis Date = 03/09/17 Pct Recovery = 118% Analysis Date = 03/09/17 Pct Recovery = 118% Analysis Date = 03/08/17 Pct Recovery = 118% Analysis Date = 03/08/17 Pct Recovery = 118% Analysis Date = 03/07/17 Pct Recovery = 118% Analysis Date = 03/07/17 Pct Recovery = 118% Analysis Date = 03/05/17 Pct Recovery = 118% Analysis Date = 03/05/17 Pct Recovery = 118% Analysis Date = 03/04/17 Pct Recovery = 118% Analysis Date = 03/04/17 Pct Recovery = 118% Analysis Date = 03/03/17 Pct Recovery = 118% Analysis Date = 03/03/17 Pct Recovery = 118% Analysis Date = 03/02/17 Pct Recovery = 118% Analysis Date = 03/02/17 Pct Recovery = 118% Analysis Date = 03/01/17 Pct Recovery = 118% Analysis Date = 03/01/17 Pct Recovery = 118% Analysis Date = 02/28/17 Pct Recovery = 118% Analysis Date = 02/28/17 Pct Recovery = 118% Analysis Date = 02/27/17 Pct Recovery = 118% Analysis Date = 02/27/17 Pct Recovery = 118% Analysis Date = 02/26/17 Pct Recovery = 118% Analysis Date = 02/26/17 Pct Recovery = 118% Analysis Date = 02/24/17 Pct Recovery = 118% Analysis Date = 02/24/17 Pct Recovery = 118% Analysis Date = 02/23/17 Pct Recovery = 118% Analysis Date = 02/23/17 Pct Recovery = 118% Analysis Date = 02/22/17 Pct Recovery = 118% Analysis Date = 02/22/17 Pct Recovery = 118% Analysis Date = 02/21/17 Pct Recovery = 118% Analysis Date = 02/21/17 Pct Recovery = 118% Analysis Date = 02/20/17 Pct Recovery = 118% Analysis Date = 02/20/17 Pct Recovery = 118% Analysis Date = 02/19/17 Pct Recovery = 118% Analysis Date = 02/19/17 Pct Recovery = 118% Analysis Date = 02/18/17 Pct Recovery = 118% Analysis Date = 02/18/17 Pct Recovery = 118% Analysis Date = 02/17/17 Pct Recovery = 118% Analysis Date = 02/17/17 Pct Recovery = 118% Analysis Date = 02/15/17 Pct Recovery = 118% Analysis Date = 02/15/17 Pct Recovery = 118% Analysis Date = 02/14/17 Pct Recovery = 118% Analysis Date = 02/14/17 Pct Recovery = 118% Analysis Date = 02/13/17 Pct Recovery = 118% Analysis Date = 02/13/17 Pct Recovery = 118% Analysis Date = 02/12/17 Pct Recovery = 118% Analysis Date = 02/12/17 Pct Recovery = 118% Analysis Date = 02/11/17 Pct Recovery = 118% Analysis Date = 02/11/17 Pct Recovery = 118% Analysis Date = 02/10/17 Pct Recovery = 118% Analysis Date = 02/10/17 Pct Recovery = 118% Analysis Date = 02/09/17 Pct Recovery = 118% Analysis Date = 02/09/17 Pct Recovery = 118% Analysis Date = 02/08/17 Pct Recovery = 118% Analysis Date = 02/08/17 Pct Recovery = 118% Analysis Date = 02/06/17 Pct Recovery = 118% Analysis Date = 02/06/17 Pct Recovery = 118% Analysis Date = 02/05/17 Pct Recovery = 119% Analysis Date = 02/05/17 Pct Recovery = 119% Analysis Date = 02/04/17 Pct Recovery = 119% Analysis Date = 02/04/17 Pct Recovery = 119% Analysis Date = 02/03/17 Pct Recovery = 119% Analysis Date = 02/03/17 Pct Recovery = 119% Analysis Date = 02/02/17 Pct Recovery = 119% Analysis Date = 02/02/17 Pct Recovery = 119% Analysis Date = 02/01/17 Pct Recovery = 119% Analysis Date = 02/01/17 Pct Recovery = 119% Analysis Date = 01/31/17 Pct Recovery = 119% Analysis Date = 01/31/17 Pct Recovery = 119% Analysis Date = 01/30/17 Pct Recovery = 119% Analysis Date = 01/30/17 Pct Recovery = 119% Analysis Date = 01/28/17 Pct Recovery = 119% Analysis Date = 01/28/17 Pct Recovery = 119% Analysis Date = 01/27/17 Pct Recovery = 119% Analysis Date = 01/27/17 Pct Recovery = 119% Analysis Date = 01/26/17 Pct Recovery = 119% Analysis Date = 01/26/17 Pct Recovery = 119% Analysis Date = 01/25/17 Pct Recovery = 119% Analysis Date = 01/25/17 Pct Recovery = 119% Analysis Date = 01/24/17 Pct Recovery = 119% Analysis Date = 01/24/17 Pct Recovery = 119% Analysis Date = 01/23/17 Pct Recovery = 119% Analysis Date = 01/23/17 Pct Recovery = 119% Analysis Date = 01/22/17 Pct Recovery = 119% Analysis Date = 01/22/17 Pct Recovery = 119% Analysis Date = 01/21/17 Pct Recovery = 119% Analysis Date = 01/21/17 Pct Recovery = 119% Analysis Date = 01/19/17 Pct Recovery = 119% Analysis Date = 01/19/17 Pct Recovery = 119% Analysis Date = 01/18/17 Pct Recovery = 119% Analysis Date = 01/18/17 Pct Recovery = 119% Analysis Date = 01/17/17 Pct Recovery = 119% Analysis Date = 01/17/17 Pct Recovery = 119% Analysis Date = 01/16/17 Pct Recovery = 119% Analysis Date = 01/16/17 Pct Recovery = 119% Analysis Date = 01/15/17 Pct Recovery = 119% Analysis Date = 01/15/17 Pct Recovery = 119% Analysis Date = 01/14/17 Pct Recovery = 119% Analysis Date = 01/14/17 Pct Recovery = 119% Analysis Date = 01/13/17 Pct Recovery = 119% Analysis Date = 01/13/17 Pct Recovery = 119% Analysis Date = 01/12/17 Pct Recovery = 119% Analysis Date = 01/12/17 Pct Recovery = 119% Analysis Date = 01/10/17 Pct Recovery = 119% Analysis Date = 01/10/17 Pct Recovery = 119% Analysis Date = 01/09/17 Pct Recovery = 119% Analysis Date = 01/09/17 Pct Recovery = 119% Analysis Date = 01/08/17 Pct Recovery = 119% Analysis Date = 01/08/17 Pct Recovery = 119% Analysis Date = 01/07/17 Pct Recovery = 119% Analysis Date = 01/07/17 Pct Recovery = 119% Analysis Date = 01/06/17 Pct Recovery = 119% Analysis Date = 01/06/17 Pct Recovery = 119% Analysis Date = 01/05/17 Pct Recovery = 120% Analysis Date = 01/05/17 Pct Recovery = 120% Analysis Date = 01/04/17 Pct Recovery = 120% Analysis Date = 01/04/17 Pct Recovery = 120% Analysis Date = 01/03/17 Pct Recovery = 120% Analysis Date = 01/03/17 Pct Recovery = 120% Analysis Date = 01/01/17 Pct Recovery = 120% Analysis Date = 01/01/17 Pct Recovery = 120% Analysis Date = 12/31/16 Pct Recovery = 120% Analysis Date = 12/31/16 Pct Recovery = 120% Analysis Date = 12/30/16 Pct Recovery = 120% Analysis Date = 12/30/16 Pct Recovery = 120% Analysis Date = 12/29/16 Pct Recovery = 120% Analysis Date = 12/29/16 Pct Recovery = 120% Analysis Date = 12/28/16 Pct Recovery = 120% Analysis Date = 12/28/16 Pct Recovery = 120% Analysis Date = 12/27/16 Pct Recovery = 120% Analysis Date = 12/27/16 Pct Recovery = 120% Analysis Date = 12/26/16 Pct Recovery = 120% Analysis Date = 12/26/16 Pct Recovery = 120% Analysis Date = 12/25/16 Pct Recovery = 120% Analysis Date = 12/25/16 Pct Recovery = 120% Analysis Date = 12/23/16 Pct Recovery = 120% Analysis Date = 12/23/16 Pct Recovery = 120% Analysis Date = 12/22/16 Pct Recovery = 120% Analysis Date = 12/22/16 Pct Recovery = 120% Analysis Date = 12/21/16 Pct Recovery = 120% Analysis Date = 12/21/16 Pct Recovery = 120% Analysis Date = 12/20/16 Pct Recovery = 120% Analysis Date = 12/20/16 Pct Recovery = 120% Analysis Date = 12/19/16 Pct Recovery = 120% Analysis Date = 12/19/16 Pct Recovery = 120% Analysis Date = 12/18/16 Pct Recovery = 120% Analysis Date = 12/18/16 Pct Recovery = 120% Analysis Date = 12/17/16 Pct Recovery = 120% Analysis Date = 12/17/16 Pct Recovery = 120% Analysis Date = 12/16/16 Pct Recovery = 120% Analysis Date = 12/16/16 Pct Recovery = 120% Analysis Date = 12/14/16 Pct Recovery = 120% Analysis Date = 12/14/16 Pct Recovery = 120% Analysis Date = 12/13/16 Pct Recovery = 120% Analysis Date = 12/13/16 Pct Recovery = 120% Analysis Date = 12/12/16 Pct Recovery = 120% Analysis Date = 12/12/16 Pct Recovery = 120% Analysis Date = 12/11/16 Pct Recovery = 120% Analysis Date = 12/11/16 Pct Recovery = 120% Analysis Date = 12/10/16 Pct Recovery = 120% Analysis Date = 12/10/16 Pct Recovery = 120% Analysis Date = 12/09/16 Pct Recovery = 120% Analysis Date = 12/09/16 Pct Recovery = 120% Analysis Date = 12/08/16 Pct Recovery = 120% Analysis Date = 12/08/16 Pct Recovery = 120% Analysis Date = 12/07/16 Pct Recovery = 120% Analysis Date = 12/07/16 Pct Recovery = 120% Analysis Date = 12/05/16 Pct Recovery = 120% Analysis Date = 12/05/16 Pct Recovery = 120% Analysis Date = 12/04/16 Pct Recovery = 121% Analysis Date = 12/04/16 Pct Recovery = 121% Analysis Date = 12/03/16 Pct Recovery = 121% Analysis Date = 12/03/16 Pct Recovery = 121% Analysis Date = 12/02/16 Pct Recovery = 121% Analysis Date = 12/02/16 Pct Recovery = 121% Analysis Date = 12/01/16 Pct Recovery = 121% Analysis Date = 12/01/16 Pct Recovery = 121% Analysis Date = 11/30/16 Pct Recovery = 121% Analysis Date = 11/30/16 Pct Recovery = 121% Analysis Date = 11/29/16 Pct Recovery = 121% Analysis Date = 11/29/16 Pct Recovery = 121% Analysis Date = 11/28/16 Pct Recovery = 121% Analysis Date = 11/28/16 Pct Recovery = 121% Analysis Date = 11/26/16 Pct Recovery = 121% Analysis Date = 11/26/16 Pct Recovery = 121% Analysis Date = 11/25/16 Pct Recovery = 121% Analysis Date = 11/25/16 Pct Recovery = 121% Analysis Date = 11/24/16 Pct Recovery = 121% Analysis Date = 11/24/16 Pct Recovery = 121% Analysis Date = 11/23/16 Pct Recovery = 121% Analysis Date = 11/23/16 Pct Recovery = 121% Analysis Date = 11/22/16 Pct Recovery = 121% Analysis Date = 11/22/16 Pct Recovery = 121% Analysis Date = 11/21/16 Pct Recovery = 121% Analysis Date = 11/21/16 Pct Recovery = 121% Analysis Date = 11/20/16 Pct Recovery = 121% Analysis Date = 11/20/16 Pct Recovery = 121% Analysis Date = 11/19/16 Pct Recovery = 121% Analysis Date = 11/19/16 Pct Recovery = 121% Analysis Date = 11/17/16 Pct Recovery = 121% Analysis Date = 11/17/16 Pct Recovery = 121% Analysis Date = 11/16/16 Pct Recovery = 121% Analysis Date = 11/16/16 Pct Recovery = 121% Analysis Date = 11/15/16 Pct Recovery = 121% Analysis Date = 11/15/16 Pct Recovery = 121% Analysis Date = 11/14/16 Pct Recovery = 121% Analysis Date = 11/14/16 Pct Recovery = 121% Analysis Date = 11/13/16 Pct Recovery = 121% Analysis Date = 11/13/16 Pct Recovery = 121% Analysis Date = 11/12/16 Pct Recovery = 121% Analysis Date = 11/12/16 Pct Recovery = 121% Analysis Date = 11/11/16 Pct Recovery = 121% Analysis Date = 11/11/16 Pct Recovery = 121% Analysis Date = 11/10/16 Pct Recovery = 121% Analysis Date = 11/10/16 Pct Recovery = 121% Analysis Date = 11/08/16 Pct Recovery = 121% Analysis Date = 11/08/16 Pct Recovery = 121% Analysis Date = 11/07/16 Pct Recovery = 121% Analysis Date = 11/07/16 Pct Recovery = 121% Analysis Date = 11/06/16 Pct Recovery = 121% Analysis Date = 11/06/16 Pct Recovery = 121% Analysis Date = 11/05/16 Pct Recovery = 121% Analysis Date = 11/05/16 Pct Recovery = 121% Analysis Date = 11/04/16 Pct Recovery = 121% Analysis Date = 11/04/16 Pct Recovery = 121% Analysis Date = 11/03/16 Pct Recovery = 122% Analysis Date = 11/03/16 Pct Recovery = 122% Analysis Date = 11/02/16 Pct Recovery = 122% Analysis Date = 11/02/16 Pct Recovery = 122% Analysis Date = 11/01/16 Pct Recovery = 122% Analysis Date = 11/01/16 Pct Recovery = 122% Analysis Date = 10/30/16 Pct Recovery = 122% Analysis Date = 10/30/16 Pct Recovery = 122% Analysis Date = 10/29/16 Pct Recovery = 122% Analysis Date = 10/29/16 Pct Recovery = 122% Analysis Date = 10/28/16 Pct Recovery = 122% Analysis Date = 10/28/16 Pct Recovery = 122% Analysis Date = 10/27/16 Pct Recovery = 122% Analysis Date = 10/27/16 Pct Recovery = 122% Analysis Date = 10/26/16 Pct Recovery = 122% Analysis Date = 10/26/16 Pct Recovery = 122% Analysis Date = 10/25/16 Pct Recovery = 122% Analysis Date = 10/25/16 Pct Recovery = 122% Analysis Date = 10/24/16 Pct Recovery = 122% Analysis Date = 10/24/16 Pct Recovery = 122% Analysis Date = 10/23/16 Pct Recovery = 122% Analysis Date = 10/23/16 Pct Recovery = 122% Analysis Date = 10/21/16 Pct Recovery = 122% Analysis Date = 10/21/16 Pct Recovery = 122% Analysis Date = 10/20/16 Pct Recovery = 122% Analysis Date = 10/20/16 Pct Recovery = 122% Analysis Date = 10/19/16 Pct Recovery = 122% Analysis Date = 10/19/16 Pct Recovery = 122% Analysis Date = 10/18/16 Pct Recovery = 121% Analysis Date = 10/18/16 Pct Recovery = 121% Analysis Date = 10/17/16 Pct Recovery = 121% Analysis Date = 10/17/16 Pct Recovery = 121% Analysis Date = 10/16/16 Pct Recovery = 120% Analysis Date = 10/16/16 Pct Recovery = 120% Analysis Date = 10/15/16 Pct Recovery = 120% Analysis Date = 10/15/16 Pct Recovery = 120% Analysis Date = 10/14/16 Pct Recovery = 119% Analysis Date = 10/14/16 Pct Recovery = 119% Analysis Date = 10/12/16 Pct Recovery = 119% Analysis Date = 10/12/16 Pct Recovery = 119% Analysis Date = 10/11/16 Pct Recovery = 118% Analysis Date = 10/11/16 Pct Recovery = 118% Analysis Date = 10/10/16 Pct Recovery = 117% Analysis Date = 10/10/16 Pct Recovery = 117% Analysis Date = 10/09/16 Pct Recovery = 117% Analysis Date = 10/09/16 Pct Recovery = 117% Analysis Date = 10/08/16 Pct Recovery = 116% Analysis Date = 10/08/16 Pct Recovery = 116% Analysis Date = 10/07/16 Pct Recovery = 116% Analysis Date = 10/07/16 Pct Recovery = 116% Analysis Date = 10/06/16 Pct Recovery = 115% Analysis Date = 10/06/16 Pct Recovery = 115% Analysis Date = 10/05/16 Pct Recovery = 115% Analysis Date = 10/05/16 Pct Recovery = 115% Analysis Date = 10/03/16 Pct Recovery = 114% Analysis Date = 10/03/16 Pct Recovery = 114% Analysis Date = 10/02/16 Pct Recovery = 114% Analysis Date = 10/02/16 Pct Recovery = 114% Analysis Date = 10/01/16 Pct Recovery = 113% Analysis Date = 10/01/16 Pct Recovery = 113% Analysis Date = 09/30/16 Pct Recovery = 113% Analysis Date = 09/30/16 Pct Recovery = 113% Analysis Date = 09/29/16 Pct Recovery = 112% Analysis Date = 09/29/16 Pct Recovery = 112% Analysis Date = 09/28/16 Pct Recovery = 111% Analysis Date = 09/28/16 Pct Recovery = 111% Analysis Date = 09/27/16 Pct Recovery = 111% Analysis Date = 09/27/16 Pct Recovery = 111% Analysis Date = 09/26/16 Pct Recovery = 110% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
CHOLESTEROL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 5 114% 11% 116% 9%
Total 5 114% 11% 116% 9%

Sample Statistics
CHOLESTEROL

Characteristic N % % Basis
Plotted 5 42% Spiked
Estimated Values 1 8% Spiked
Deleted Values 1 5% Spiked + Not Spiked
Spiked, Censored 2 17% Spiked
Spiked 12 .  
False Negatives 5 42% 5 out of 12
Not Spiked 7 .  
False Positives 2 33% 2 out of 6

BQS OBSP Determination:
CIS-ANDROSTERONE
METHOD: 6434 , TESTIDCODE: 63607GM006
Open Data Set

Analysis Date = 09/26/16 SpikeMix = Abs 051616sed4H1: 0 µl & Abs 051616sed4L2: 0 µl Pct Recovery = 54% Analysis Date = 09/26/16 SpikeMix = Abs 051616sed4H3: 0 µl & Abs 051616sed4H1: 0 µl Pct Recovery = 52% Analysis Date = 09/26/16 SpikeMix = Abs 051616sed4H1: 0 µl & Abs 051616sed4H2: 0 µl Pct Recovery = 52% Analysis Date = 05/24/17 SpikeMix = ERA 04121614: 0 µl & Abs 051616sed4L: 0 µl Pct Recovery = 56% Analysis Date = 04/19/17 SpikeMix = ERA 04121613: 0 µl & ERA 04121614: 0 µl Pct Recovery = 60% Analysis Date = 03/17/17 SpikeMix = ERA 04121615: 0 µl & ERA 04121613: 0 µl Pct Recovery = 50% Analysis Date = 05/24/17 Pct Recovery = 56% Analysis Date = 05/22/17 Pct Recovery = 56% Analysis Date = 05/22/17 Pct Recovery = 56% Analysis Date = 05/21/17 Pct Recovery = 56% Analysis Date = 05/21/17 Pct Recovery = 56% Analysis Date = 05/20/17 Pct Recovery = 56% Analysis Date = 05/20/17 Pct Recovery = 56% Analysis Date = 05/19/17 Pct Recovery = 57% Analysis Date = 05/19/17 Pct Recovery = 57% Analysis Date = 05/18/17 Pct Recovery = 57% Analysis Date = 05/18/17 Pct Recovery = 57% Analysis Date = 05/16/17 Pct Recovery = 57% Analysis Date = 05/16/17 Pct Recovery = 57% Analysis Date = 05/15/17 Pct Recovery = 57% Analysis Date = 05/15/17 Pct Recovery = 57% Analysis Date = 05/14/17 Pct Recovery = 57% Analysis Date = 05/14/17 Pct Recovery = 57% Analysis Date = 05/13/17 Pct Recovery = 57% Analysis Date = 05/13/17 Pct Recovery = 57% Analysis Date = 05/12/17 Pct Recovery = 57% Analysis Date = 05/12/17 Pct Recovery = 57% Analysis Date = 05/10/17 Pct Recovery = 58% Analysis Date = 05/10/17 Pct Recovery = 58% Analysis Date = 05/09/17 Pct Recovery = 58% Analysis Date = 05/09/17 Pct Recovery = 58% Analysis Date = 05/08/17 Pct Recovery = 58% Analysis Date = 05/08/17 Pct Recovery = 58% Analysis Date = 05/07/17 Pct Recovery = 58% Analysis Date = 05/07/17 Pct Recovery = 58% Analysis Date = 05/06/17 Pct Recovery = 58% Analysis Date = 05/06/17 Pct Recovery = 58% Analysis Date = 05/04/17 Pct Recovery = 58% Analysis Date = 05/04/17 Pct Recovery = 58% Analysis Date = 05/03/17 Pct Recovery = 58% Analysis Date = 05/03/17 Pct Recovery = 58% Analysis Date = 05/02/17 Pct Recovery = 59% Analysis Date = 05/02/17 Pct Recovery = 59% Analysis Date = 05/01/17 Pct Recovery = 59% Analysis Date = 05/01/17 Pct Recovery = 59% Analysis Date = 04/30/17 Pct Recovery = 59% Analysis Date = 04/30/17 Pct Recovery = 59% Analysis Date = 04/28/17 Pct Recovery = 59% Analysis Date = 04/28/17 Pct Recovery = 59% Analysis Date = 04/27/17 Pct Recovery = 59% Analysis Date = 04/27/17 Pct Recovery = 59% Analysis Date = 04/26/17 Pct Recovery = 59% Analysis Date = 04/26/17 Pct Recovery = 59% Analysis Date = 04/25/17 Pct Recovery = 59% Analysis Date = 04/25/17 Pct Recovery = 59% Analysis Date = 04/24/17 Pct Recovery = 60% Analysis Date = 04/24/17 Pct Recovery = 60% Analysis Date = 04/22/17 Pct Recovery = 60% Analysis Date = 04/22/17 Pct Recovery = 60% Analysis Date = 04/21/17 Pct Recovery = 60% Analysis Date = 04/21/17 Pct Recovery = 60% Analysis Date = 04/20/17 Pct Recovery = 60% Analysis Date = 04/20/17 Pct Recovery = 60% Analysis Date = 04/19/17 Pct Recovery = 60% Analysis Date = 04/19/17 Pct Recovery = 60% Analysis Date = 04/18/17 Pct Recovery = 60% Analysis Date = 04/18/17 Pct Recovery = 60% Analysis Date = 04/16/17 Pct Recovery = 60% Analysis Date = 04/16/17 Pct Recovery = 60% Analysis Date = 04/15/17 Pct Recovery = 59% Analysis Date = 04/15/17 Pct Recovery = 59% Analysis Date = 04/14/17 Pct Recovery = 59% Analysis Date = 04/14/17 Pct Recovery = 59% Analysis Date = 04/13/17 Pct Recovery = 58% Analysis Date = 04/13/17 Pct Recovery = 58% Analysis Date = 04/12/17 Pct Recovery = 58% Analysis Date = 04/12/17 Pct Recovery = 58% Analysis Date = 04/10/17 Pct Recovery = 58% Analysis Date = 04/10/17 Pct Recovery = 58% Analysis Date = 04/09/17 Pct Recovery = 57% Analysis Date = 04/09/17 Pct Recovery = 57% Analysis Date = 04/08/17 Pct Recovery = 57% Analysis Date = 04/08/17 Pct Recovery = 57% Analysis Date = 04/07/17 Pct Recovery = 57% Analysis Date = 04/07/17 Pct Recovery = 57% Analysis Date = 04/06/17 Pct Recovery = 56% Analysis Date = 04/06/17 Pct Recovery = 56% Analysis Date = 04/04/17 Pct Recovery = 56% Analysis Date = 04/04/17 Pct Recovery = 56% Analysis Date = 04/03/17 Pct Recovery = 56% Analysis Date = 04/03/17 Pct Recovery = 56% Analysis Date = 04/02/17 Pct Recovery = 55% Analysis Date = 04/02/17 Pct Recovery = 55% Analysis Date = 04/01/17 Pct Recovery = 55% Analysis Date = 04/01/17 Pct Recovery = 55% Analysis Date = 03/31/17 Pct Recovery = 54% Analysis Date = 03/31/17 Pct Recovery = 54% Analysis Date = 03/29/17 Pct Recovery = 54% Analysis Date = 03/29/17 Pct Recovery = 54% Analysis Date = 03/28/17 Pct Recovery = 54% Analysis Date = 03/28/17 Pct Recovery = 54% Analysis Date = 03/27/17 Pct Recovery = 53% Analysis Date = 03/27/17 Pct Recovery = 53% Analysis Date = 03/26/17 Pct Recovery = 53% Analysis Date = 03/26/17 Pct Recovery = 53% Analysis Date = 03/25/17 Pct Recovery = 53% Analysis Date = 03/25/17 Pct Recovery = 53% Analysis Date = 03/23/17 Pct Recovery = 52% Analysis Date = 03/23/17 Pct Recovery = 52% Analysis Date = 03/22/17 Pct Recovery = 52% Analysis Date = 03/22/17 Pct Recovery = 52% Analysis Date = 03/21/17 Pct Recovery = 52% Analysis Date = 03/21/17 Pct Recovery = 52% Analysis Date = 03/20/17 Pct Recovery = 51% Analysis Date = 03/20/17 Pct Recovery = 51% Analysis Date = 03/19/17 Pct Recovery = 51% Analysis Date = 03/19/17 Pct Recovery = 51% Analysis Date = 03/17/17 Pct Recovery = 50% Analysis Date = 03/17/17 Pct Recovery = 50% Analysis Date = 03/16/17 Pct Recovery = 50% Analysis Date = 03/16/17 Pct Recovery = 50% Analysis Date = 03/15/17 Pct Recovery = 50% Analysis Date = 03/15/17 Pct Recovery = 50% Analysis Date = 03/14/17 Pct Recovery = 50% Analysis Date = 03/14/17 Pct Recovery = 50% Analysis Date = 03/13/17 Pct Recovery = 50% Analysis Date = 03/13/17 Pct Recovery = 50% Analysis Date = 03/11/17 Pct Recovery = 50% Analysis Date = 03/11/17 Pct Recovery = 50% Analysis Date = 03/10/17 Pct Recovery = 50% Analysis Date = 03/10/17 Pct Recovery = 50% Analysis Date = 03/09/17 Pct Recovery = 50% Analysis Date = 03/09/17 Pct Recovery = 50% Analysis Date = 03/08/17 Pct Recovery = 50% Analysis Date = 03/08/17 Pct Recovery = 50% Analysis Date = 03/07/17 Pct Recovery = 50% Analysis Date = 03/07/17 Pct Recovery = 50% Analysis Date = 03/05/17 Pct Recovery = 50% Analysis Date = 03/05/17 Pct Recovery = 50% Analysis Date = 03/04/17 Pct Recovery = 50% Analysis Date = 03/04/17 Pct Recovery = 50% Analysis Date = 03/03/17 Pct Recovery = 50% Analysis Date = 03/03/17 Pct Recovery = 50% Analysis Date = 03/02/17 Pct Recovery = 50% Analysis Date = 03/02/17 Pct Recovery = 50% Analysis Date = 03/01/17 Pct Recovery = 50% Analysis Date = 03/01/17 Pct Recovery = 50% Analysis Date = 02/27/17 Pct Recovery = 50% Analysis Date = 02/27/17 Pct Recovery = 50% Analysis Date = 02/26/17 Pct Recovery = 50% Analysis Date = 02/26/17 Pct Recovery = 50% Analysis Date = 02/25/17 Pct Recovery = 51% Analysis Date = 02/25/17 Pct Recovery = 51% Analysis Date = 02/24/17 Pct Recovery = 51% Analysis Date = 02/24/17 Pct Recovery = 51% Analysis Date = 02/23/17 Pct Recovery = 51% Analysis Date = 02/23/17 Pct Recovery = 51% Analysis Date = 02/21/17 Pct Recovery = 51% Analysis Date = 02/21/17 Pct Recovery = 51% Analysis Date = 02/20/17 Pct Recovery = 51% Analysis Date = 02/20/17 Pct Recovery = 51% Analysis Date = 02/19/17 Pct Recovery = 51% Analysis Date = 02/19/17 Pct Recovery = 51% Analysis Date = 02/18/17 Pct Recovery = 51% Analysis Date = 02/18/17 Pct Recovery = 51% Analysis Date = 02/17/17 Pct Recovery = 51% Analysis Date = 02/17/17 Pct Recovery = 51% Analysis Date = 02/15/17 Pct Recovery = 51% Analysis Date = 02/15/17 Pct Recovery = 51% Analysis Date = 02/14/17 Pct Recovery = 51% Analysis Date = 02/14/17 Pct Recovery = 51% Analysis Date = 02/13/17 Pct Recovery = 51% Analysis Date = 02/13/17 Pct Recovery = 51% Analysis Date = 02/12/17 Pct Recovery = 51% Analysis Date = 02/12/17 Pct Recovery = 51% Analysis Date = 02/11/17 Pct Recovery = 51% Analysis Date = 02/11/17 Pct Recovery = 51% Analysis Date = 02/09/17 Pct Recovery = 51% Analysis Date = 02/09/17 Pct Recovery = 51% Analysis Date = 02/08/17 Pct Recovery = 51% Analysis Date = 02/08/17 Pct Recovery = 51% Analysis Date = 02/07/17 Pct Recovery = 51% Analysis Date = 02/07/17 Pct Recovery = 51% Analysis Date = 02/06/17 Pct Recovery = 51% Analysis Date = 02/06/17 Pct Recovery = 51% Analysis Date = 02/05/17 Pct Recovery = 51% Analysis Date = 02/05/17 Pct Recovery = 51% Analysis Date = 02/03/17 Pct Recovery = 51% Analysis Date = 02/03/17 Pct Recovery = 51% Analysis Date = 02/02/17 Pct Recovery = 51% Analysis Date = 02/02/17 Pct Recovery = 51% Analysis Date = 02/01/17 Pct Recovery = 51% Analysis Date = 02/01/17 Pct Recovery = 51% Analysis Date = 01/31/17 Pct Recovery = 51% Analysis Date = 01/31/17 Pct Recovery = 51% Analysis Date = 01/30/17 Pct Recovery = 51% Analysis Date = 01/30/17 Pct Recovery = 51% Analysis Date = 01/28/17 Pct Recovery = 51% Analysis Date = 01/28/17 Pct Recovery = 51% Analysis Date = 01/27/17 Pct Recovery = 51% Analysis Date = 01/27/17 Pct Recovery = 51% Analysis Date = 01/26/17 Pct Recovery = 51% Analysis Date = 01/26/17 Pct Recovery = 51% Analysis Date = 01/25/17 Pct Recovery = 51% Analysis Date = 01/25/17 Pct Recovery = 51% Analysis Date = 01/24/17 Pct Recovery = 51% Analysis Date = 01/24/17 Pct Recovery = 51% Analysis Date = 01/22/17 Pct Recovery = 51% Analysis Date = 01/22/17 Pct Recovery = 51% Analysis Date = 01/21/17 Pct Recovery = 51% Analysis Date = 01/21/17 Pct Recovery = 51% Analysis Date = 01/20/17 Pct Recovery = 51% Analysis Date = 01/20/17 Pct Recovery = 51% Analysis Date = 01/19/17 Pct Recovery = 51% Analysis Date = 01/19/17 Pct Recovery = 51% Analysis Date = 01/18/17 Pct Recovery = 51% Analysis Date = 01/18/17 Pct Recovery = 51% Analysis Date = 01/16/17 Pct Recovery = 51% Analysis Date = 01/16/17 Pct Recovery = 51% Analysis Date = 01/15/17 Pct Recovery = 51% Analysis Date = 01/15/17 Pct Recovery = 51% Analysis Date = 01/14/17 Pct Recovery = 51% Analysis Date = 01/14/17 Pct Recovery = 51% Analysis Date = 01/13/17 Pct Recovery = 51% Analysis Date = 01/13/17 Pct Recovery = 51% Analysis Date = 01/12/17 Pct Recovery = 51% Analysis Date = 01/12/17 Pct Recovery = 51% Analysis Date = 01/10/17 Pct Recovery = 51% Analysis Date = 01/10/17 Pct Recovery = 51% Analysis Date = 01/09/17 Pct Recovery = 51% Analysis Date = 01/09/17 Pct Recovery = 51% Analysis Date = 01/08/17 Pct Recovery = 51% Analysis Date = 01/08/17 Pct Recovery = 51% Analysis Date = 01/07/17 Pct Recovery = 51% Analysis Date = 01/07/17 Pct Recovery = 51% Analysis Date = 01/06/17 Pct Recovery = 51% Analysis Date = 01/06/17 Pct Recovery = 51% Analysis Date = 01/04/17 Pct Recovery = 51% Analysis Date = 01/04/17 Pct Recovery = 51% Analysis Date = 01/03/17 Pct Recovery = 51% Analysis Date = 01/03/17 Pct Recovery = 51% Analysis Date = 01/02/17 Pct Recovery = 51% Analysis Date = 01/02/17 Pct Recovery = 51% Analysis Date = 01/01/17 Pct Recovery = 51% Analysis Date = 01/01/17 Pct Recovery = 51% Analysis Date = 12/31/16 Pct Recovery = 51% Analysis Date = 12/31/16 Pct Recovery = 51% Analysis Date = 12/29/16 Pct Recovery = 51% Analysis Date = 12/29/16 Pct Recovery = 51% Analysis Date = 12/28/16 Pct Recovery = 51% Analysis Date = 12/28/16 Pct Recovery = 51% Analysis Date = 12/27/16 Pct Recovery = 51% Analysis Date = 12/27/16 Pct Recovery = 51% Analysis Date = 12/26/16 Pct Recovery = 51% Analysis Date = 12/26/16 Pct Recovery = 51% Analysis Date = 12/25/16 Pct Recovery = 51% Analysis Date = 12/25/16 Pct Recovery = 51% Analysis Date = 12/23/16 Pct Recovery = 52% Analysis Date = 12/23/16 Pct Recovery = 52% Analysis Date = 12/22/16 Pct Recovery = 52% Analysis Date = 12/22/16 Pct Recovery = 52% Analysis Date = 12/21/16 Pct Recovery = 52% Analysis Date = 12/21/16 Pct Recovery = 52% Analysis Date = 12/20/16 Pct Recovery = 52% Analysis Date = 12/20/16 Pct Recovery = 52% Analysis Date = 12/19/16 Pct Recovery = 52% Analysis Date = 12/19/16 Pct Recovery = 52% Analysis Date = 12/17/16 Pct Recovery = 52% Analysis Date = 12/17/16 Pct Recovery = 52% Analysis Date = 12/16/16 Pct Recovery = 52% Analysis Date = 12/16/16 Pct Recovery = 52% Analysis Date = 12/15/16 Pct Recovery = 52% Analysis Date = 12/15/16 Pct Recovery = 52% Analysis Date = 12/14/16 Pct Recovery = 52% Analysis Date = 12/14/16 Pct Recovery = 52% Analysis Date = 12/13/16 Pct Recovery = 52% Analysis Date = 12/13/16 Pct Recovery = 52% Analysis Date = 12/11/16 Pct Recovery = 52% Analysis Date = 12/11/16 Pct Recovery = 52% Analysis Date = 12/10/16 Pct Recovery = 52% Analysis Date = 12/10/16 Pct Recovery = 52% Analysis Date = 12/09/16 Pct Recovery = 52% Analysis Date = 12/09/16 Pct Recovery = 52% Analysis Date = 12/08/16 Pct Recovery = 52% Analysis Date = 12/08/16 Pct Recovery = 52% Analysis Date = 12/07/16 Pct Recovery = 52% Analysis Date = 12/07/16 Pct Recovery = 52% Analysis Date = 12/05/16 Pct Recovery = 52% Analysis Date = 12/05/16 Pct Recovery = 52% Analysis Date = 12/04/16 Pct Recovery = 52% Analysis Date = 12/04/16 Pct Recovery = 52% Analysis Date = 12/03/16 Pct Recovery = 52% Analysis Date = 12/03/16 Pct Recovery = 52% Analysis Date = 12/02/16 Pct Recovery = 52% Analysis Date = 12/02/16 Pct Recovery = 52% Analysis Date = 12/01/16 Pct Recovery = 52% Analysis Date = 12/01/16 Pct Recovery = 52% Analysis Date = 11/29/16 Pct Recovery = 52% Analysis Date = 11/29/16 Pct Recovery = 52% Analysis Date = 11/28/16 Pct Recovery = 52% Analysis Date = 11/28/16 Pct Recovery = 52% Analysis Date = 11/27/16 Pct Recovery = 52% Analysis Date = 11/27/16 Pct Recovery = 52% Analysis Date = 11/26/16 Pct Recovery = 52% Analysis Date = 11/26/16 Pct Recovery = 52% Analysis Date = 11/25/16 Pct Recovery = 52% Analysis Date = 11/25/16 Pct Recovery = 52% Analysis Date = 11/23/16 Pct Recovery = 52% Analysis Date = 11/23/16 Pct Recovery = 52% Analysis Date = 11/22/16 Pct Recovery = 52% Analysis Date = 11/22/16 Pct Recovery = 52% Analysis Date = 11/21/16 Pct Recovery = 52% Analysis Date = 11/21/16 Pct Recovery = 52% Analysis Date = 11/20/16 Pct Recovery = 52% Analysis Date = 11/20/16 Pct Recovery = 52% Analysis Date = 11/19/16 Pct Recovery = 52% Analysis Date = 11/19/16 Pct Recovery = 52% Analysis Date = 11/17/16 Pct Recovery = 52% Analysis Date = 11/17/16 Pct Recovery = 52% Analysis Date = 11/16/16 Pct Recovery = 52% Analysis Date = 11/16/16 Pct Recovery = 52% Analysis Date = 11/15/16 Pct Recovery = 52% Analysis Date = 11/15/16 Pct Recovery = 52% Analysis Date = 11/14/16 Pct Recovery = 52% Analysis Date = 11/14/16 Pct Recovery = 52% Analysis Date = 11/13/16 Pct Recovery = 52% Analysis Date = 11/13/16 Pct Recovery = 52% Analysis Date = 11/11/16 Pct Recovery = 52% Analysis Date = 11/11/16 Pct Recovery = 52% Analysis Date = 11/10/16 Pct Recovery = 52% Analysis Date = 11/10/16 Pct Recovery = 52% Analysis Date = 11/09/16 Pct Recovery = 52% Analysis Date = 11/09/16 Pct Recovery = 52% Analysis Date = 11/08/16 Pct Recovery = 52% Analysis Date = 11/08/16 Pct Recovery = 52% Analysis Date = 11/07/16 Pct Recovery = 52% Analysis Date = 11/07/16 Pct Recovery = 52% Analysis Date = 11/05/16 Pct Recovery = 52% Analysis Date = 11/05/16 Pct Recovery = 52% Analysis Date = 11/04/16 Pct Recovery = 52% Analysis Date = 11/04/16 Pct Recovery = 52% Analysis Date = 11/03/16 Pct Recovery = 52% Analysis Date = 11/03/16 Pct Recovery = 52% Analysis Date = 11/02/16 Pct Recovery = 52% Analysis Date = 11/02/16 Pct Recovery = 52% Analysis Date = 11/01/16 Pct Recovery = 52% Analysis Date = 11/01/16 Pct Recovery = 52% Analysis Date = 10/30/16 Pct Recovery = 52% Analysis Date = 10/30/16 Pct Recovery = 52% Analysis Date = 10/29/16 Pct Recovery = 52% Analysis Date = 10/29/16 Pct Recovery = 52% Analysis Date = 10/28/16 Pct Recovery = 52% Analysis Date = 10/28/16 Pct Recovery = 52% Analysis Date = 10/27/16 Pct Recovery = 52% Analysis Date = 10/27/16 Pct Recovery = 52% Analysis Date = 10/26/16 Pct Recovery = 52% Analysis Date = 10/26/16 Pct Recovery = 52% Analysis Date = 10/24/16 Pct Recovery = 52% Analysis Date = 10/24/16 Pct Recovery = 52% Analysis Date = 10/23/16 Pct Recovery = 52% Analysis Date = 10/23/16 Pct Recovery = 52% Analysis Date = 10/22/16 Pct Recovery = 52% Analysis Date = 10/22/16 Pct Recovery = 52% Analysis Date = 10/21/16 Pct Recovery = 53% Analysis Date = 10/21/16 Pct Recovery = 53% Analysis Date = 10/20/16 Pct Recovery = 53% Analysis Date = 10/20/16 Pct Recovery = 53% Analysis Date = 10/18/16 Pct Recovery = 53% Analysis Date = 10/18/16 Pct Recovery = 53% Analysis Date = 10/17/16 Pct Recovery = 53% Analysis Date = 10/17/16 Pct Recovery = 53% Analysis Date = 10/16/16 Pct Recovery = 53% Analysis Date = 10/16/16 Pct Recovery = 53% Analysis Date = 10/15/16 Pct Recovery = 53% Analysis Date = 10/15/16 Pct Recovery = 53% Analysis Date = 10/14/16 Pct Recovery = 53% Analysis Date = 10/14/16 Pct Recovery = 53% Analysis Date = 10/12/16 Pct Recovery = 53% Analysis Date = 10/12/16 Pct Recovery = 53% Analysis Date = 10/11/16 Pct Recovery = 53% Analysis Date = 10/11/16 Pct Recovery = 53% Analysis Date = 10/10/16 Pct Recovery = 53% Analysis Date = 10/10/16 Pct Recovery = 53% Analysis Date = 10/09/16 Pct Recovery = 53% Analysis Date = 10/09/16 Pct Recovery = 53% Analysis Date = 10/08/16 Pct Recovery = 53% Analysis Date = 10/08/16 Pct Recovery = 53% Analysis Date = 10/06/16 Pct Recovery = 53% Analysis Date = 10/06/16 Pct Recovery = 53% Analysis Date = 10/05/16 Pct Recovery = 53% Analysis Date = 10/05/16 Pct Recovery = 53% Analysis Date = 10/04/16 Pct Recovery = 53% Analysis Date = 10/04/16 Pct Recovery = 53% Analysis Date = 10/03/16 Pct Recovery = 53% Analysis Date = 10/03/16 Pct Recovery = 53% Analysis Date = 10/02/16 Pct Recovery = 53% Analysis Date = 10/02/16 Pct Recovery = 53% Analysis Date = 09/30/16 Pct Recovery = 53% Analysis Date = 09/30/16 Pct Recovery = 53% Analysis Date = 09/29/16 Pct Recovery = 53% Analysis Date = 09/29/16 Pct Recovery = 53% Analysis Date = 09/28/16 Pct Recovery = 53% Analysis Date = 09/28/16 Pct Recovery = 53% Analysis Date = 09/27/16 Pct Recovery = 53% Analysis Date = 09/27/16 Pct Recovery = 53% Analysis Date = 09/26/16 Pct Recovery = 53% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
CIS-ANDROSTERONE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 2 55% 7% 55% 7%
>= Reporting Level 4 54% 2% 53% 2%
Total 6 54% 4% 53% 3%

Sample Statistics
CIS-ANDROSTERONE

Characteristic N % % Basis
Plotted 6 50% Spiked
Estimated Values 0 0% Spiked
Deleted Values 1 5% Spiked + Not Spiked
Spiked, Censored 5 42% Spiked
Spiked 12 .  
False Negatives 1 8% 1 out of 12
Not Spiked 7 .  
False Positives 0 0% 0 out of 6

BQS OBSP Determination:
DIHYDROTESTOSTERONE
METHOD: 6434 , TESTIDCODE: 64484GM006
Open Data Set

Analysis Date = 09/26/16 SpikeMix = Abs 051616sed4H3: 0 µl & Abs 051616sed4H1: 0 µl Pct Recovery = 74% Analysis Date = 05/09/17 SpikeMix = ERA 04121615: 0 µl & Abs 051616sed4L: 0 µl Pct Recovery = 120% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
DIHYDROTESTOSTERONE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 2 97% 32% 97% 34%
Total 2 97% 32% 97% 34%

Sample Statistics
DIHYDROTESTOSTERONE

Characteristic N % % Basis
Plotted 2 33% Spiked
Estimated Values 0 0% Spiked
Deleted Values 1 5% Spiked + Not Spiked
Spiked, Censored 4 67% Spiked
Spiked 6 .  
False Negatives 0 0% 0 out of 6
Not Spiked 13 .  
False Positives 0 0% 0 out of 12

BQS OBSP Determination:
EPITESTOSTERONE
METHOD: 6434 , TESTIDCODE: 64477GM006
Open Data Set

Analysis Date = 09/26/16 SpikeMix = Abs 051616sed4H1: 0 µl & Abs 051616sed4L2: 0 µl Pct Recovery = 81% Analysis Date = 09/26/16 SpikeMix = Abs 051616sed4H3: 0 µl & Abs 051616sed4H1: 0 µl Pct Recovery = 48% Analysis Date = 09/26/16 SpikeMix = Abs 051616sed4H1: 0 µl & Abs 051616sed4H2: 0 µl Pct Recovery = 49% Analysis Date = 05/24/17 SpikeMix = ERA 04121614: 0 µl & Abs 051616sed4L: 0 µl Pct Recovery = 33% Analysis Date = 05/24/17 SpikeMix = ERA 04121613: 0 µl Pct Recovery = 175% Analysis Date = 05/09/17 SpikeMix = ERA 04121615: 0 µl & Abs 051616sed4L: 0 µl Pct Recovery = 54% Analysis Date = 04/28/17 SpikeMix = ERA 04121615: 0 µl & ERA 04121613: 0 µl Pct Recovery = 71% Analysis Date = 04/19/17 SpikeMix = ERA 04121613: 0 µl & ERA 04121614: 0 µl Pct Recovery = 60% Analysis Date = 03/17/17 SpikeMix = ERA 04121613: 0 µl & ERA 04121614: 0 µl Pct Recovery = 46% Analysis Date = 10/20/16 SpikeMix = Abs 051616sed4H3: 0 µl & Abs 051616sed4L: 0 µl Pct Recovery = 79% Analysis Date = 05/24/17 Pct Recovery = 98% Analysis Date = 05/22/17 Pct Recovery = 97% Analysis Date = 05/22/17 Pct Recovery = 97% Analysis Date = 05/21/17 Pct Recovery = 95% Analysis Date = 05/21/17 Pct Recovery = 95% Analysis Date = 05/20/17 Pct Recovery = 93% Analysis Date = 05/20/17 Pct Recovery = 93% Analysis Date = 05/19/17 Pct Recovery = 92% Analysis Date = 05/19/17 Pct Recovery = 92% Analysis Date = 05/18/17 Pct Recovery = 90% Analysis Date = 05/18/17 Pct Recovery = 90% Analysis Date = 05/16/17 Pct Recovery = 89% Analysis Date = 05/16/17 Pct Recovery = 89% Analysis Date = 05/15/17 Pct Recovery = 87% Analysis Date = 05/15/17 Pct Recovery = 87% Analysis Date = 05/14/17 Pct Recovery = 85% Analysis Date = 05/14/17 Pct Recovery = 85% Analysis Date = 05/13/17 Pct Recovery = 84% Analysis Date = 05/13/17 Pct Recovery = 84% Analysis Date = 05/12/17 Pct Recovery = 82% Analysis Date = 05/12/17 Pct Recovery = 82% Analysis Date = 05/10/17 Pct Recovery = 81% Analysis Date = 05/10/17 Pct Recovery = 81% Analysis Date = 05/09/17 Pct Recovery = 79% Analysis Date = 05/09/17 Pct Recovery = 79% Analysis Date = 05/08/17 Pct Recovery = 78% Analysis Date = 05/08/17 Pct Recovery = 78% Analysis Date = 05/07/17 Pct Recovery = 76% Analysis Date = 05/07/17 Pct Recovery = 76% Analysis Date = 05/06/17 Pct Recovery = 75% Analysis Date = 05/06/17 Pct Recovery = 75% Analysis Date = 05/04/17 Pct Recovery = 73% Analysis Date = 05/04/17 Pct Recovery = 73% Analysis Date = 05/03/17 Pct Recovery = 72% Analysis Date = 05/03/17 Pct Recovery = 72% Analysis Date = 05/02/17 Pct Recovery = 70% Analysis Date = 05/02/17 Pct Recovery = 70% Analysis Date = 05/01/17 Pct Recovery = 69% Analysis Date = 05/01/17 Pct Recovery = 69% Analysis Date = 04/30/17 Pct Recovery = 67% Analysis Date = 04/30/17 Pct Recovery = 67% Analysis Date = 04/28/17 Pct Recovery = 66% Analysis Date = 04/28/17 Pct Recovery = 66% Analysis Date = 04/27/17 Pct Recovery = 64% Analysis Date = 04/27/17 Pct Recovery = 64% Analysis Date = 04/26/17 Pct Recovery = 64% Analysis Date = 04/26/17 Pct Recovery = 64% Analysis Date = 04/25/17 Pct Recovery = 64% Analysis Date = 04/25/17 Pct Recovery = 64% Analysis Date = 04/24/17 Pct Recovery = 64% Analysis Date = 04/24/17 Pct Recovery = 64% Analysis Date = 04/22/17 Pct Recovery = 64% Analysis Date = 04/22/17 Pct Recovery = 64% Analysis Date = 04/21/17 Pct Recovery = 64% Analysis Date = 04/21/17 Pct Recovery = 64% Analysis Date = 04/20/17 Pct Recovery = 64% Analysis Date = 04/20/17 Pct Recovery = 64% Analysis Date = 04/19/17 Pct Recovery = 64% Analysis Date = 04/19/17 Pct Recovery = 64% Analysis Date = 04/18/17 Pct Recovery = 63% Analysis Date = 04/18/17 Pct Recovery = 63% Analysis Date = 04/16/17 Pct Recovery = 62% Analysis Date = 04/16/17 Pct Recovery = 62% Analysis Date = 04/15/17 Pct Recovery = 62% Analysis Date = 04/15/17 Pct Recovery = 62% Analysis Date = 04/14/17 Pct Recovery = 61% Analysis Date = 04/14/17 Pct Recovery = 61% Analysis Date = 04/13/17 Pct Recovery = 61% Analysis Date = 04/13/17 Pct Recovery = 61% Analysis Date = 04/12/17 Pct Recovery = 60% Analysis Date = 04/12/17 Pct Recovery = 60% Analysis Date = 04/10/17 Pct Recovery = 59% Analysis Date = 04/10/17 Pct Recovery = 59% Analysis Date = 04/09/17 Pct Recovery = 59% Analysis Date = 04/09/17 Pct Recovery = 59% Analysis Date = 04/08/17 Pct Recovery = 58% Analysis Date = 04/08/17 Pct Recovery = 58% Analysis Date = 04/07/17 Pct Recovery = 58% Analysis Date = 04/07/17 Pct Recovery = 58% Analysis Date = 04/06/17 Pct Recovery = 57% Analysis Date = 04/06/17 Pct Recovery = 57% Analysis Date = 04/04/17 Pct Recovery = 56% Analysis Date = 04/04/17 Pct Recovery = 56% Analysis Date = 04/03/17 Pct Recovery = 56% Analysis Date = 04/03/17 Pct Recovery = 56% Analysis Date = 04/02/17 Pct Recovery = 55% Analysis Date = 04/02/17 Pct Recovery = 55% Analysis Date = 04/01/17 Pct Recovery = 55% Analysis Date = 04/01/17 Pct Recovery = 55% Analysis Date = 03/31/17 Pct Recovery = 54% Analysis Date = 03/31/17 Pct Recovery = 54% Analysis Date = 03/29/17 Pct Recovery = 53% Analysis Date = 03/29/17 Pct Recovery = 53% Analysis Date = 03/28/17 Pct Recovery = 53% Analysis Date = 03/28/17 Pct Recovery = 53% Analysis Date = 03/27/17 Pct Recovery = 52% Analysis Date = 03/27/17 Pct Recovery = 52% Analysis Date = 03/26/17 Pct Recovery = 52% Analysis Date = 03/26/17 Pct Recovery = 52% Analysis Date = 03/25/17 Pct Recovery = 51% Analysis Date = 03/25/17 Pct Recovery = 51% Analysis Date = 03/23/17 Pct Recovery = 50% Analysis Date = 03/23/17 Pct Recovery = 50% Analysis Date = 03/22/17 Pct Recovery = 50% Analysis Date = 03/22/17 Pct Recovery = 50% Analysis Date = 03/21/17 Pct Recovery = 49% Analysis Date = 03/21/17 Pct Recovery = 49% Analysis Date = 03/20/17 Pct Recovery = 48% Analysis Date = 03/20/17 Pct Recovery = 48% Analysis Date = 03/19/17 Pct Recovery = 48% Analysis Date = 03/19/17 Pct Recovery = 48% Analysis Date = 03/17/17 Pct Recovery = 47% Analysis Date = 03/17/17 Pct Recovery = 47% Analysis Date = 03/16/17 Pct Recovery = 47% Analysis Date = 03/16/17 Pct Recovery = 47% Analysis Date = 03/15/17 Pct Recovery = 47% Analysis Date = 03/15/17 Pct Recovery = 47% Analysis Date = 03/14/17 Pct Recovery = 47% Analysis Date = 03/14/17 Pct Recovery = 47% Analysis Date = 03/13/17 Pct Recovery = 47% Analysis Date = 03/13/17 Pct Recovery = 47% Analysis Date = 03/11/17 Pct Recovery = 47% Analysis Date = 03/11/17 Pct Recovery = 47% Analysis Date = 03/10/17 Pct Recovery = 48% Analysis Date = 03/10/17 Pct Recovery = 48% Analysis Date = 03/09/17 Pct Recovery = 48% Analysis Date = 03/09/17 Pct Recovery = 48% Analysis Date = 03/08/17 Pct Recovery = 48% Analysis Date = 03/08/17 Pct Recovery = 48% Analysis Date = 03/07/17 Pct Recovery = 48% Analysis Date = 03/07/17 Pct Recovery = 48% Analysis Date = 03/05/17 Pct Recovery = 48% Analysis Date = 03/05/17 Pct Recovery = 48% Analysis Date = 03/04/17 Pct Recovery = 48% Analysis Date = 03/04/17 Pct Recovery = 48% Analysis Date = 03/03/17 Pct Recovery = 48% Analysis Date = 03/03/17 Pct Recovery = 48% Analysis Date = 03/02/17 Pct Recovery = 49% Analysis Date = 03/02/17 Pct Recovery = 49% Analysis Date = 03/01/17 Pct Recovery = 49% Analysis Date = 03/01/17 Pct Recovery = 49% Analysis Date = 02/27/17 Pct Recovery = 49% Analysis Date = 02/27/17 Pct Recovery = 49% Analysis Date = 02/26/17 Pct Recovery = 49% Analysis Date = 02/26/17 Pct Recovery = 49% Analysis Date = 02/25/17 Pct Recovery = 49% Analysis Date = 02/25/17 Pct Recovery = 49% Analysis Date = 02/24/17 Pct Recovery = 49% Analysis Date = 02/24/17 Pct Recovery = 49% Analysis Date = 02/23/17 Pct Recovery = 49% Analysis Date = 02/23/17 Pct Recovery = 49% Analysis Date = 02/21/17 Pct Recovery = 50% Analysis Date = 02/21/17 Pct Recovery = 50% Analysis Date = 02/20/17 Pct Recovery = 50% Analysis Date = 02/20/17 Pct Recovery = 50% Analysis Date = 02/19/17 Pct Recovery = 50% Analysis Date = 02/19/17 Pct Recovery = 50% Analysis Date = 02/18/17 Pct Recovery = 50% Analysis Date = 02/18/17 Pct Recovery = 50% Analysis Date = 02/17/17 Pct Recovery = 50% Analysis Date = 02/17/17 Pct Recovery = 50% Analysis Date = 02/15/17 Pct Recovery = 50% Analysis Date = 02/15/17 Pct Recovery = 50% Analysis Date = 02/14/17 Pct Recovery = 50% Analysis Date = 02/14/17 Pct Recovery = 50% Analysis Date = 02/13/17 Pct Recovery = 51% Analysis Date = 02/13/17 Pct Recovery = 51% Analysis Date = 02/12/17 Pct Recovery = 51% Analysis Date = 02/12/17 Pct Recovery = 51% Analysis Date = 02/11/17 Pct Recovery = 51% Analysis Date = 02/11/17 Pct Recovery = 51% Analysis Date = 02/09/17 Pct Recovery = 51% Analysis Date = 02/09/17 Pct Recovery = 51% Analysis Date = 02/08/17 Pct Recovery = 51% Analysis Date = 02/08/17 Pct Recovery = 51% Analysis Date = 02/07/17 Pct Recovery = 51% Analysis Date = 02/07/17 Pct Recovery = 51% Analysis Date = 02/06/17 Pct Recovery = 51% Analysis Date = 02/06/17 Pct Recovery = 51% Analysis Date = 02/05/17 Pct Recovery = 52% Analysis Date = 02/05/17 Pct Recovery = 52% Analysis Date = 02/03/17 Pct Recovery = 52% Analysis Date = 02/03/17 Pct Recovery = 52% Analysis Date = 02/02/17 Pct Recovery = 52% Analysis Date = 02/02/17 Pct Recovery = 52% Analysis Date = 02/01/17 Pct Recovery = 52% Analysis Date = 02/01/17 Pct Recovery = 52% Analysis Date = 01/31/17 Pct Recovery = 52% Analysis Date = 01/31/17 Pct Recovery = 52% Analysis Date = 01/30/17 Pct Recovery = 52% Analysis Date = 01/30/17 Pct Recovery = 52% Analysis Date = 01/28/17 Pct Recovery = 52% Analysis Date = 01/28/17 Pct Recovery = 52% Analysis Date = 01/27/17 Pct Recovery = 53% Analysis Date = 01/27/17 Pct Recovery = 53% Analysis Date = 01/26/17 Pct Recovery = 53% Analysis Date = 01/26/17 Pct Recovery = 53% Analysis Date = 01/25/17 Pct Recovery = 53% Analysis Date = 01/25/17 Pct Recovery = 53% Analysis Date = 01/24/17 Pct Recovery = 53% Analysis Date = 01/24/17 Pct Recovery = 53% Analysis Date = 01/22/17 Pct Recovery = 53% Analysis Date = 01/22/17 Pct Recovery = 53% Analysis Date = 01/21/17 Pct Recovery = 53% Analysis Date = 01/21/17 Pct Recovery = 53% Analysis Date = 01/20/17 Pct Recovery = 53% Analysis Date = 01/20/17 Pct Recovery = 53% Analysis Date = 01/19/17 Pct Recovery = 54% Analysis Date = 01/19/17 Pct Recovery = 54% Analysis Date = 01/18/17 Pct Recovery = 54% Analysis Date = 01/18/17 Pct Recovery = 54% Analysis Date = 01/16/17 Pct Recovery = 54% Analysis Date = 01/16/17 Pct Recovery = 54% Analysis Date = 01/15/17 Pct Recovery = 54% Analysis Date = 01/15/17 Pct Recovery = 54% Analysis Date = 01/14/17 Pct Recovery = 54% Analysis Date = 01/14/17 Pct Recovery = 54% Analysis Date = 01/13/17 Pct Recovery = 54% Analysis Date = 01/13/17 Pct Recovery = 54% Analysis Date = 01/12/17 Pct Recovery = 54% Analysis Date = 01/12/17 Pct Recovery = 54% Analysis Date = 01/10/17 Pct Recovery = 55% Analysis Date = 01/10/17 Pct Recovery = 55% Analysis Date = 01/09/17 Pct Recovery = 55% Analysis Date = 01/09/17 Pct Recovery = 55% Analysis Date = 01/08/17 Pct Recovery = 55% Analysis Date = 01/08/17 Pct Recovery = 55% Analysis Date = 01/07/17 Pct Recovery = 55% Analysis Date = 01/07/17 Pct Recovery = 55% Analysis Date = 01/06/17 Pct Recovery = 55% Analysis Date = 01/06/17 Pct Recovery = 55% Analysis Date = 01/04/17 Pct Recovery = 55% Analysis Date = 01/04/17 Pct Recovery = 55% Analysis Date = 01/03/17 Pct Recovery = 55% Analysis Date = 01/03/17 Pct Recovery = 55% Analysis Date = 01/02/17 Pct Recovery = 56% Analysis Date = 01/02/17 Pct Recovery = 56% Analysis Date = 01/01/17 Pct Recovery = 56% Analysis Date = 01/01/17 Pct Recovery = 56% Analysis Date = 12/31/16 Pct Recovery = 56% Analysis Date = 12/31/16 Pct Recovery = 56% Analysis Date = 12/29/16 Pct Recovery = 56% Analysis Date = 12/29/16 Pct Recovery = 56% Analysis Date = 12/28/16 Pct Recovery = 56% Analysis Date = 12/28/16 Pct Recovery = 56% Analysis Date = 12/27/16 Pct Recovery = 56% Analysis Date = 12/27/16 Pct Recovery = 56% Analysis Date = 12/26/16 Pct Recovery = 56% Analysis Date = 12/26/16 Pct Recovery = 56% Analysis Date = 12/25/16 Pct Recovery = 57% Analysis Date = 12/25/16 Pct Recovery = 57% Analysis Date = 12/23/16 Pct Recovery = 57% Analysis Date = 12/23/16 Pct Recovery = 57% Analysis Date = 12/22/16 Pct Recovery = 57% Analysis Date = 12/22/16 Pct Recovery = 57% Analysis Date = 12/21/16 Pct Recovery = 57% Analysis Date = 12/21/16 Pct Recovery = 57% Analysis Date = 12/20/16 Pct Recovery = 57% Analysis Date = 12/20/16 Pct Recovery = 57% Analysis Date = 12/19/16 Pct Recovery = 57% Analysis Date = 12/19/16 Pct Recovery = 57% Analysis Date = 12/17/16 Pct Recovery = 57% Analysis Date = 12/17/16 Pct Recovery = 57% Analysis Date = 12/16/16 Pct Recovery = 57% Analysis Date = 12/16/16 Pct Recovery = 57% Analysis Date = 12/15/16 Pct Recovery = 58% Analysis Date = 12/15/16 Pct Recovery = 58% Analysis Date = 12/14/16 Pct Recovery = 58% Analysis Date = 12/14/16 Pct Recovery = 58% Analysis Date = 12/13/16 Pct Recovery = 58% Analysis Date = 12/13/16 Pct Recovery = 58% Analysis Date = 12/11/16 Pct Recovery = 58% Analysis Date = 12/11/16 Pct Recovery = 58% Analysis Date = 12/10/16 Pct Recovery = 58% Analysis Date = 12/10/16 Pct Recovery = 58% Analysis Date = 12/09/16 Pct Recovery = 58% Analysis Date = 12/09/16 Pct Recovery = 58% Analysis Date = 12/08/16 Pct Recovery = 58% Analysis Date = 12/08/16 Pct Recovery = 58% Analysis Date = 12/07/16 Pct Recovery = 59% Analysis Date = 12/07/16 Pct Recovery = 59% Analysis Date = 12/05/16 Pct Recovery = 59% Analysis Date = 12/05/16 Pct Recovery = 59% Analysis Date = 12/04/16 Pct Recovery = 59% Analysis Date = 12/04/16 Pct Recovery = 59% Analysis Date = 12/03/16 Pct Recovery = 59% Analysis Date = 12/03/16 Pct Recovery = 59% Analysis Date = 12/02/16 Pct Recovery = 59% Analysis Date = 12/02/16 Pct Recovery = 59% Analysis Date = 12/01/16 Pct Recovery = 59% Analysis Date = 12/01/16 Pct Recovery = 59% Analysis Date = 11/29/16 Pct Recovery = 59% Analysis Date = 11/29/16 Pct Recovery = 59% Analysis Date = 11/28/16 Pct Recovery = 60% Analysis Date = 11/28/16 Pct Recovery = 60% Analysis Date = 11/27/16 Pct Recovery = 60% Analysis Date = 11/27/16 Pct Recovery = 60% Analysis Date = 11/26/16 Pct Recovery = 60% Analysis Date = 11/26/16 Pct Recovery = 60% Analysis Date = 11/25/16 Pct Recovery = 60% Analysis Date = 11/25/16 Pct Recovery = 60% Analysis Date = 11/23/16 Pct Recovery = 60% Analysis Date = 11/23/16 Pct Recovery = 60% Analysis Date = 11/22/16 Pct Recovery = 60% Analysis Date = 11/22/16 Pct Recovery = 60% Analysis Date = 11/21/16 Pct Recovery = 60% Analysis Date = 11/21/16 Pct Recovery = 60% Analysis Date = 11/20/16 Pct Recovery = 61% Analysis Date = 11/20/16 Pct Recovery = 61% Analysis Date = 11/19/16 Pct Recovery = 61% Analysis Date = 11/19/16 Pct Recovery = 61% Analysis Date = 11/17/16 Pct Recovery = 61% Analysis Date = 11/17/16 Pct Recovery = 61% Analysis Date = 11/16/16 Pct Recovery = 61% Analysis Date = 11/16/16 Pct Recovery = 61% Analysis Date = 11/15/16 Pct Recovery = 61% Analysis Date = 11/15/16 Pct Recovery = 61% Analysis Date = 11/14/16 Pct Recovery = 61% Analysis Date = 11/14/16 Pct Recovery = 61% Analysis Date = 11/13/16 Pct Recovery = 61% Analysis Date = 11/13/16 Pct Recovery = 61% Analysis Date = 11/11/16 Pct Recovery = 62% Analysis Date = 11/11/16 Pct Recovery = 62% Analysis Date = 11/10/16 Pct Recovery = 62% Analysis Date = 11/10/16 Pct Recovery = 62% Analysis Date = 11/09/16 Pct Recovery = 62% Analysis Date = 11/09/16 Pct Recovery = 62% Analysis Date = 11/08/16 Pct Recovery = 62% Analysis Date = 11/08/16 Pct Recovery = 62% Analysis Date = 11/07/16 Pct Recovery = 62% Analysis Date = 11/07/16 Pct Recovery = 62% Analysis Date = 11/05/16 Pct Recovery = 62% Analysis Date = 11/05/16 Pct Recovery = 62% Analysis Date = 11/04/16 Pct Recovery = 62% Analysis Date = 11/04/16 Pct Recovery = 62% Analysis Date = 11/03/16 Pct Recovery = 63% Analysis Date = 11/03/16 Pct Recovery = 63% Analysis Date = 11/02/16 Pct Recovery = 63% Analysis Date = 11/02/16 Pct Recovery = 63% Analysis Date = 11/01/16 Pct Recovery = 63% Analysis Date = 11/01/16 Pct Recovery = 63% Analysis Date = 10/30/16 Pct Recovery = 63% Analysis Date = 10/30/16 Pct Recovery = 63% Analysis Date = 10/29/16 Pct Recovery = 63% Analysis Date = 10/29/16 Pct Recovery = 63% Analysis Date = 10/28/16 Pct Recovery = 63% Analysis Date = 10/28/16 Pct Recovery = 63% Analysis Date = 10/27/16 Pct Recovery = 63% Analysis Date = 10/27/16 Pct Recovery = 63% Analysis Date = 10/26/16 Pct Recovery = 64% Analysis Date = 10/26/16 Pct Recovery = 64% Analysis Date = 10/24/16 Pct Recovery = 64% Analysis Date = 10/24/16 Pct Recovery = 64% Analysis Date = 10/23/16 Pct Recovery = 64% Analysis Date = 10/23/16 Pct Recovery = 64% Analysis Date = 10/22/16 Pct Recovery = 64% Analysis Date = 10/22/16 Pct Recovery = 64% Analysis Date = 10/21/16 Pct Recovery = 64% Analysis Date = 10/21/16 Pct Recovery = 64% Analysis Date = 10/20/16 Pct Recovery = 64% Analysis Date = 10/20/16 Pct Recovery = 64% Analysis Date = 10/18/16 Pct Recovery = 64% Analysis Date = 10/18/16 Pct Recovery = 64% Analysis Date = 10/17/16 Pct Recovery = 64% Analysis Date = 10/17/16 Pct Recovery = 64% Analysis Date = 10/16/16 Pct Recovery = 64% Analysis Date = 10/16/16 Pct Recovery = 64% Analysis Date = 10/15/16 Pct Recovery = 64% Analysis Date = 10/15/16 Pct Recovery = 64% Analysis Date = 10/14/16 Pct Recovery = 64% Analysis Date = 10/14/16 Pct Recovery = 64% Analysis Date = 10/12/16 Pct Recovery = 64% Analysis Date = 10/12/16 Pct Recovery = 64% Analysis Date = 10/11/16 Pct Recovery = 64% Analysis Date = 10/11/16 Pct Recovery = 64% Analysis Date = 10/10/16 Pct Recovery = 64% Analysis Date = 10/10/16 Pct Recovery = 64% Analysis Date = 10/09/16 Pct Recovery = 64% Analysis Date = 10/09/16 Pct Recovery = 64% Analysis Date = 10/08/16 Pct Recovery = 64% Analysis Date = 10/08/16 Pct Recovery = 64% Analysis Date = 10/06/16 Pct Recovery = 64% Analysis Date = 10/06/16 Pct Recovery = 64% Analysis Date = 10/05/16 Pct Recovery = 64% Analysis Date = 10/05/16 Pct Recovery = 64% Analysis Date = 10/04/16 Pct Recovery = 64% Analysis Date = 10/04/16 Pct Recovery = 64% Analysis Date = 10/03/16 Pct Recovery = 64% Analysis Date = 10/03/16 Pct Recovery = 64% Analysis Date = 10/02/16 Pct Recovery = 63% Analysis Date = 10/02/16 Pct Recovery = 63% Analysis Date = 09/30/16 Pct Recovery = 63% Analysis Date = 09/30/16 Pct Recovery = 63% Analysis Date = 09/29/16 Pct Recovery = 63% Analysis Date = 09/29/16 Pct Recovery = 63% Analysis Date = 09/28/16 Pct Recovery = 63% Analysis Date = 09/28/16 Pct Recovery = 63% Analysis Date = 09/27/16 Pct Recovery = 63% Analysis Date = 09/27/16 Pct Recovery = 63% Analysis Date = 09/26/16 Pct Recovery = 63% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
EPITESTOSTERONE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 10 70% 40% 57% 24%
Total 10 70% 40% 57% 24%

Sample Statistics
EPITESTOSTERONE

Characteristic N % % Basis
Plotted 10 83% Spiked
Estimated Values 3 25% Spiked
Deleted Values 1 5% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 12 .  
False Negatives 2 17% 2 out of 12
Not Spiked 7 .  
False Positives 0 0% 0 out of 6

BQS OBSP Determination:
EQUILENIN
METHOD: 6434 , TESTIDCODE: 63204GM006
Open Data Set

Analysis Date = 09/26/16 SpikeMix = Abs 051616sed4H1: 0 µl & Abs 051616sed4L2: 0 µl Pct Recovery = 241% Analysis Date = 09/26/16 SpikeMix = Abs 051616sed4H3: 0 µl & Abs 051616sed4H1: 0 µl Pct Recovery = 51% Analysis Date = 09/26/16 SpikeMix = Abs 051616sed4H1: 0 µl & Abs 051616sed4H2: 0 µl Pct Recovery = 150% Analysis Date = 04/19/17 SpikeMix = ERA 04121613: 0 µl & ERA 04121614: 0 µl Pct Recovery = 26% Analysis Date = 04/19/17 Pct Recovery = 26% Analysis Date = 04/17/17 Pct Recovery = 27% Analysis Date = 04/17/17 Pct Recovery = 27% Analysis Date = 04/16/17 Pct Recovery = 27% Analysis Date = 04/16/17 Pct Recovery = 27% Analysis Date = 04/15/17 Pct Recovery = 27% Analysis Date = 04/15/17 Pct Recovery = 27% Analysis Date = 04/14/17 Pct Recovery = 28% Analysis Date = 04/14/17 Pct Recovery = 28% Analysis Date = 04/13/17 Pct Recovery = 28% Analysis Date = 04/13/17 Pct Recovery = 28% Analysis Date = 04/12/17 Pct Recovery = 28% Analysis Date = 04/12/17 Pct Recovery = 28% Analysis Date = 04/11/17 Pct Recovery = 29% Analysis Date = 04/11/17 Pct Recovery = 29% Analysis Date = 04/10/17 Pct Recovery = 29% Analysis Date = 04/10/17 Pct Recovery = 29% Analysis Date = 04/09/17 Pct Recovery = 29% Analysis Date = 04/09/17 Pct Recovery = 29% Analysis Date = 04/08/17 Pct Recovery = 30% Analysis Date = 04/08/17 Pct Recovery = 30% Analysis Date = 04/07/17 Pct Recovery = 30% Analysis Date = 04/07/17 Pct Recovery = 30% Analysis Date = 04/06/17 Pct Recovery = 31% Analysis Date = 04/06/17 Pct Recovery = 31% Analysis Date = 04/05/17 Pct Recovery = 31% Analysis Date = 04/05/17 Pct Recovery = 31% Analysis Date = 04/04/17 Pct Recovery = 31% Analysis Date = 04/04/17 Pct Recovery = 31% Analysis Date = 04/03/17 Pct Recovery = 32% Analysis Date = 04/03/17 Pct Recovery = 32% Analysis Date = 04/02/17 Pct Recovery = 32% Analysis Date = 04/02/17 Pct Recovery = 32% Analysis Date = 04/01/17 Pct Recovery = 32% Analysis Date = 04/01/17 Pct Recovery = 32% Analysis Date = 03/31/17 Pct Recovery = 33% Analysis Date = 03/31/17 Pct Recovery = 33% Analysis Date = 03/30/17 Pct Recovery = 33% Analysis Date = 03/30/17 Pct Recovery = 33% Analysis Date = 03/29/17 Pct Recovery = 34% Analysis Date = 03/29/17 Pct Recovery = 34% Analysis Date = 03/28/17 Pct Recovery = 34% Analysis Date = 03/28/17 Pct Recovery = 34% Analysis Date = 03/27/17 Pct Recovery = 34% Analysis Date = 03/27/17 Pct Recovery = 34% Analysis Date = 03/26/17 Pct Recovery = 35% Analysis Date = 03/26/17 Pct Recovery = 35% Analysis Date = 03/25/17 Pct Recovery = 35% Analysis Date = 03/25/17 Pct Recovery = 35% Analysis Date = 03/24/17 Pct Recovery = 35% Analysis Date = 03/24/17 Pct Recovery = 35% Analysis Date = 03/23/17 Pct Recovery = 36% Analysis Date = 03/23/17 Pct Recovery = 36% Analysis Date = 03/22/17 Pct Recovery = 36% Analysis Date = 03/22/17 Pct Recovery = 36% Analysis Date = 03/21/17 Pct Recovery = 37% Analysis Date = 03/21/17 Pct Recovery = 37% Analysis Date = 03/20/17 Pct Recovery = 37% Analysis Date = 03/20/17 Pct Recovery = 37% Analysis Date = 03/19/17 Pct Recovery = 37% Analysis Date = 03/19/17 Pct Recovery = 37% Analysis Date = 03/18/17 Pct Recovery = 38% Analysis Date = 03/18/17 Pct Recovery = 38% Analysis Date = 03/17/17 Pct Recovery = 38% Analysis Date = 03/17/17 Pct Recovery = 38% Analysis Date = 03/16/17 Pct Recovery = 38% Analysis Date = 03/16/17 Pct Recovery = 38% Analysis Date = 03/15/17 Pct Recovery = 39% Analysis Date = 03/15/17 Pct Recovery = 39% Analysis Date = 03/14/17 Pct Recovery = 39% Analysis Date = 03/14/17 Pct Recovery = 39% Analysis Date = 03/13/17 Pct Recovery = 40% Analysis Date = 03/13/17 Pct Recovery = 40% Analysis Date = 03/12/17 Pct Recovery = 40% Analysis Date = 03/12/17 Pct Recovery = 40% Analysis Date = 03/11/17 Pct Recovery = 40% Analysis Date = 03/11/17 Pct Recovery = 40% Analysis Date = 03/10/17 Pct Recovery = 41% Analysis Date = 03/10/17 Pct Recovery = 41% Analysis Date = 03/09/17 Pct Recovery = 41% Analysis Date = 03/09/17 Pct Recovery = 41% Analysis Date = 03/07/17 Pct Recovery = 41% Analysis Date = 03/07/17 Pct Recovery = 41% Analysis Date = 03/06/17 Pct Recovery = 42% Analysis Date = 03/06/17 Pct Recovery = 42% Analysis Date = 03/05/17 Pct Recovery = 42% Analysis Date = 03/05/17 Pct Recovery = 42% Analysis Date = 03/04/17 Pct Recovery = 43% Analysis Date = 03/04/17 Pct Recovery = 43% Analysis Date = 03/03/17 Pct Recovery = 43% Analysis Date = 03/03/17 Pct Recovery = 43% Analysis Date = 03/02/17 Pct Recovery = 43% Analysis Date = 03/02/17 Pct Recovery = 43% Analysis Date = 03/01/17 Pct Recovery = 44% Analysis Date = 03/01/17 Pct Recovery = 44% Analysis Date = 02/28/17 Pct Recovery = 44% Analysis Date = 02/28/17 Pct Recovery = 44% Analysis Date = 02/27/17 Pct Recovery = 44% Analysis Date = 02/27/17 Pct Recovery = 44% Analysis Date = 02/26/17 Pct Recovery = 45% Analysis Date = 02/26/17 Pct Recovery = 45% Analysis Date = 02/25/17 Pct Recovery = 45% Analysis Date = 02/25/17 Pct Recovery = 45% Analysis Date = 02/24/17 Pct Recovery = 45% Analysis Date = 02/24/17 Pct Recovery = 45% Analysis Date = 02/23/17 Pct Recovery = 46% Analysis Date = 02/23/17 Pct Recovery = 46% Analysis Date = 02/22/17 Pct Recovery = 46% Analysis Date = 02/22/17 Pct Recovery = 46% Analysis Date = 02/21/17 Pct Recovery = 47% Analysis Date = 02/21/17 Pct Recovery = 47% Analysis Date = 02/20/17 Pct Recovery = 47% Analysis Date = 02/20/17 Pct Recovery = 47% Analysis Date = 02/19/17 Pct Recovery = 47% Analysis Date = 02/19/17 Pct Recovery = 47% Analysis Date = 02/18/17 Pct Recovery = 48% Analysis Date = 02/18/17 Pct Recovery = 48% Analysis Date = 02/17/17 Pct Recovery = 48% Analysis Date = 02/17/17 Pct Recovery = 48% Analysis Date = 02/16/17 Pct Recovery = 48% Analysis Date = 02/16/17 Pct Recovery = 48% Analysis Date = 02/15/17 Pct Recovery = 49% Analysis Date = 02/15/17 Pct Recovery = 49% Analysis Date = 02/14/17 Pct Recovery = 49% Analysis Date = 02/14/17 Pct Recovery = 49% Analysis Date = 02/13/17 Pct Recovery = 50% Analysis Date = 02/13/17 Pct Recovery = 50% Analysis Date = 02/12/17 Pct Recovery = 50% Analysis Date = 02/12/17 Pct Recovery = 50% Analysis Date = 02/11/17 Pct Recovery = 50% Analysis Date = 02/11/17 Pct Recovery = 50% Analysis Date = 02/10/17 Pct Recovery = 51% Analysis Date = 02/10/17 Pct Recovery = 51% Analysis Date = 02/09/17 Pct Recovery = 51% Analysis Date = 02/09/17 Pct Recovery = 51% Analysis Date = 02/08/17 Pct Recovery = 51% Analysis Date = 02/08/17 Pct Recovery = 51% Analysis Date = 02/07/17 Pct Recovery = 52% Analysis Date = 02/07/17 Pct Recovery = 52% Analysis Date = 02/06/17 Pct Recovery = 52% Analysis Date = 02/06/17 Pct Recovery = 52% Analysis Date = 02/05/17 Pct Recovery = 53% Analysis Date = 02/05/17 Pct Recovery = 53% Analysis Date = 02/04/17 Pct Recovery = 53% Analysis Date = 02/04/17 Pct Recovery = 53% Analysis Date = 02/03/17 Pct Recovery = 53% Analysis Date = 02/03/17 Pct Recovery = 53% Analysis Date = 02/02/17 Pct Recovery = 54% Analysis Date = 02/02/17 Pct Recovery = 54% Analysis Date = 02/01/17 Pct Recovery = 54% Analysis Date = 02/01/17 Pct Recovery = 54% Analysis Date = 01/31/17 Pct Recovery = 54% Analysis Date = 01/31/17 Pct Recovery = 54% Analysis Date = 01/30/17 Pct Recovery = 55% Analysis Date = 01/30/17 Pct Recovery = 55% Analysis Date = 01/29/17 Pct Recovery = 55% Analysis Date = 01/29/17 Pct Recovery = 55% Analysis Date = 01/28/17 Pct Recovery = 56% Analysis Date = 01/28/17 Pct Recovery = 56% Analysis Date = 01/27/17 Pct Recovery = 56% Analysis Date = 01/27/17 Pct Recovery = 56% Analysis Date = 01/25/17 Pct Recovery = 56% Analysis Date = 01/25/17 Pct Recovery = 56% Analysis Date = 01/24/17 Pct Recovery = 57% Analysis Date = 01/24/17 Pct Recovery = 57% Analysis Date = 01/23/17 Pct Recovery = 57% Analysis Date = 01/23/17 Pct Recovery = 57% Analysis Date = 01/22/17 Pct Recovery = 57% Analysis Date = 01/22/17 Pct Recovery = 57% Analysis Date = 01/21/17 Pct Recovery = 58% Analysis Date = 01/21/17 Pct Recovery = 58% Analysis Date = 01/20/17 Pct Recovery = 58% Analysis Date = 01/20/17 Pct Recovery = 58% Analysis Date = 01/19/17 Pct Recovery = 58% Analysis Date = 01/19/17 Pct Recovery = 58% Analysis Date = 01/18/17 Pct Recovery = 59% Analysis Date = 01/18/17 Pct Recovery = 59% Analysis Date = 01/17/17 Pct Recovery = 59% Analysis Date = 01/17/17 Pct Recovery = 59% Analysis Date = 01/16/17 Pct Recovery = 60% Analysis Date = 01/16/17 Pct Recovery = 60% Analysis Date = 01/15/17 Pct Recovery = 60% Analysis Date = 01/15/17 Pct Recovery = 60% Analysis Date = 01/14/17 Pct Recovery = 60% Analysis Date = 01/14/17 Pct Recovery = 60% Analysis Date = 01/13/17 Pct Recovery = 61% Analysis Date = 01/13/17 Pct Recovery = 61% Analysis Date = 01/12/17 Pct Recovery = 61% Analysis Date = 01/12/17 Pct Recovery = 61% Analysis Date = 01/11/17 Pct Recovery = 61% Analysis Date = 01/11/17 Pct Recovery = 61% Analysis Date = 01/10/17 Pct Recovery = 62% Analysis Date = 01/10/17 Pct Recovery = 62% Analysis Date = 01/09/17 Pct Recovery = 62% Analysis Date = 01/09/17 Pct Recovery = 62% Analysis Date = 01/08/17 Pct Recovery = 63% Analysis Date = 01/08/17 Pct Recovery = 63% Analysis Date = 01/07/17 Pct Recovery = 63% Analysis Date = 01/07/17 Pct Recovery = 63% Analysis Date = 01/06/17 Pct Recovery = 63% Analysis Date = 01/06/17 Pct Recovery = 63% Analysis Date = 01/05/17 Pct Recovery = 64% Analysis Date = 01/05/17 Pct Recovery = 64% Analysis Date = 01/04/17 Pct Recovery = 64% Analysis Date = 01/04/17 Pct Recovery = 64% Analysis Date = 01/03/17 Pct Recovery = 64% Analysis Date = 01/03/17 Pct Recovery = 64% Analysis Date = 01/02/17 Pct Recovery = 65% Analysis Date = 01/02/17 Pct Recovery = 65% Analysis Date = 01/01/17 Pct Recovery = 65% Analysis Date = 01/01/17 Pct Recovery = 65% Analysis Date = 12/31/16 Pct Recovery = 66% Analysis Date = 12/31/16 Pct Recovery = 66% Analysis Date = 12/30/16 Pct Recovery = 66% Analysis Date = 12/30/16 Pct Recovery = 66% Analysis Date = 12/29/16 Pct Recovery = 66% Analysis Date = 12/29/16 Pct Recovery = 66% Analysis Date = 12/28/16 Pct Recovery = 67% Analysis Date = 12/28/16 Pct Recovery = 67% Analysis Date = 12/27/16 Pct Recovery = 67% Analysis Date = 12/27/16 Pct Recovery = 67% Analysis Date = 12/26/16 Pct Recovery = 67% Analysis Date = 12/26/16 Pct Recovery = 67% Analysis Date = 12/25/16 Pct Recovery = 68% Analysis Date = 12/25/16 Pct Recovery = 68% Analysis Date = 12/24/16 Pct Recovery = 68% Analysis Date = 12/24/16 Pct Recovery = 68% Analysis Date = 12/23/16 Pct Recovery = 69% Analysis Date = 12/23/16 Pct Recovery = 69% Analysis Date = 12/22/16 Pct Recovery = 69% Analysis Date = 12/22/16 Pct Recovery = 69% Analysis Date = 12/21/16 Pct Recovery = 69% Analysis Date = 12/21/16 Pct Recovery = 69% Analysis Date = 12/20/16 Pct Recovery = 70% Analysis Date = 12/20/16 Pct Recovery = 70% Analysis Date = 12/19/16 Pct Recovery = 70% Analysis Date = 12/19/16 Pct Recovery = 70% Analysis Date = 12/18/16 Pct Recovery = 70% Analysis Date = 12/18/16 Pct Recovery = 70% Analysis Date = 12/17/16 Pct Recovery = 71% Analysis Date = 12/17/16 Pct Recovery = 71% Analysis Date = 12/15/16 Pct Recovery = 71% Analysis Date = 12/15/16 Pct Recovery = 71% Analysis Date = 12/14/16 Pct Recovery = 71% Analysis Date = 12/14/16 Pct Recovery = 71% Analysis Date = 12/13/16 Pct Recovery = 72% Analysis Date = 12/13/16 Pct Recovery = 72% Analysis Date = 12/12/16 Pct Recovery = 72% Analysis Date = 12/12/16 Pct Recovery = 72% Analysis Date = 12/11/16 Pct Recovery = 73% Analysis Date = 12/11/16 Pct Recovery = 73% Analysis Date = 12/10/16 Pct Recovery = 73% Analysis Date = 12/10/16 Pct Recovery = 73% Analysis Date = 12/09/16 Pct Recovery = 73% Analysis Date = 12/09/16 Pct Recovery = 73% Analysis Date = 12/08/16 Pct Recovery = 74% Analysis Date = 12/08/16 Pct Recovery = 74% Analysis Date = 12/07/16 Pct Recovery = 74% Analysis Date = 12/07/16 Pct Recovery = 74% Analysis Date = 12/06/16 Pct Recovery = 74% Analysis Date = 12/06/16 Pct Recovery = 74% Analysis Date = 12/05/16 Pct Recovery = 75% Analysis Date = 12/05/16 Pct Recovery = 75% Analysis Date = 12/04/16 Pct Recovery = 75% Analysis Date = 12/04/16 Pct Recovery = 75% Analysis Date = 12/03/16 Pct Recovery = 76% Analysis Date = 12/03/16 Pct Recovery = 76% Analysis Date = 12/02/16 Pct Recovery = 76% Analysis Date = 12/02/16 Pct Recovery = 76% Analysis Date = 12/01/16 Pct Recovery = 76% Analysis Date = 12/01/16 Pct Recovery = 76% Analysis Date = 11/30/16 Pct Recovery = 77% Analysis Date = 11/30/16 Pct Recovery = 77% Analysis Date = 11/29/16 Pct Recovery = 77% Analysis Date = 11/29/16 Pct Recovery = 77% Analysis Date = 11/28/16 Pct Recovery = 77% Analysis Date = 11/28/16 Pct Recovery = 77% Analysis Date = 11/27/16 Pct Recovery = 78% Analysis Date = 11/27/16 Pct Recovery = 78% Analysis Date = 11/26/16 Pct Recovery = 78% Analysis Date = 11/26/16 Pct Recovery = 78% Analysis Date = 11/25/16 Pct Recovery = 79% Analysis Date = 11/25/16 Pct Recovery = 79% Analysis Date = 11/24/16 Pct Recovery = 79% Analysis Date = 11/24/16 Pct Recovery = 79% Analysis Date = 11/23/16 Pct Recovery = 79% Analysis Date = 11/23/16 Pct Recovery = 79% Analysis Date = 11/22/16 Pct Recovery = 80% Analysis Date = 11/22/16 Pct Recovery = 80% Analysis Date = 11/21/16 Pct Recovery = 80% Analysis Date = 11/21/16 Pct Recovery = 80% Analysis Date = 11/20/16 Pct Recovery = 80% Analysis Date = 11/20/16 Pct Recovery = 80% Analysis Date = 11/19/16 Pct Recovery = 81% Analysis Date = 11/19/16 Pct Recovery = 81% Analysis Date = 11/18/16 Pct Recovery = 81% Analysis Date = 11/18/16 Pct Recovery = 81% Analysis Date = 11/17/16 Pct Recovery = 82% Analysis Date = 11/17/16 Pct Recovery = 82% Analysis Date = 11/16/16 Pct Recovery = 82% Analysis Date = 11/16/16 Pct Recovery = 82% Analysis Date = 11/15/16 Pct Recovery = 82% Analysis Date = 11/15/16 Pct Recovery = 82% Analysis Date = 11/14/16 Pct Recovery = 83% Analysis Date = 11/14/16 Pct Recovery = 83% Analysis Date = 11/13/16 Pct Recovery = 83% Analysis Date = 11/13/16 Pct Recovery = 83% Analysis Date = 11/12/16 Pct Recovery = 83% Analysis Date = 11/12/16 Pct Recovery = 83% Analysis Date = 11/11/16 Pct Recovery = 84% Analysis Date = 11/11/16 Pct Recovery = 84% Analysis Date = 11/10/16 Pct Recovery = 84% Analysis Date = 11/10/16 Pct Recovery = 84% Analysis Date = 11/09/16 Pct Recovery = 85% Analysis Date = 11/09/16 Pct Recovery = 85% Analysis Date = 11/08/16 Pct Recovery = 85% Analysis Date = 11/08/16 Pct Recovery = 85% Analysis Date = 11/07/16 Pct Recovery = 85% Analysis Date = 11/07/16 Pct Recovery = 85% Analysis Date = 11/06/16 Pct Recovery = 86% Analysis Date = 11/06/16 Pct Recovery = 86% Analysis Date = 11/04/16 Pct Recovery = 86% Analysis Date = 11/04/16 Pct Recovery = 86% Analysis Date = 11/03/16 Pct Recovery = 86% Analysis Date = 11/03/16 Pct Recovery = 86% Analysis Date = 11/02/16 Pct Recovery = 87% Analysis Date = 11/02/16 Pct Recovery = 87% Analysis Date = 11/01/16 Pct Recovery = 87% Analysis Date = 11/01/16 Pct Recovery = 87% Analysis Date = 10/31/16 Pct Recovery = 87% Analysis Date = 10/31/16 Pct Recovery = 87% Analysis Date = 10/30/16 Pct Recovery = 88% Analysis Date = 10/30/16 Pct Recovery = 88% Analysis Date = 10/29/16 Pct Recovery = 88% Analysis Date = 10/29/16 Pct Recovery = 88% Analysis Date = 10/28/16 Pct Recovery = 89% Analysis Date = 10/28/16 Pct Recovery = 89% Analysis Date = 10/27/16 Pct Recovery = 89% Analysis Date = 10/27/16 Pct Recovery = 89% Analysis Date = 10/26/16 Pct Recovery = 89% Analysis Date = 10/26/16 Pct Recovery = 89% Analysis Date = 10/25/16 Pct Recovery = 90% Analysis Date = 10/25/16 Pct Recovery = 90% Analysis Date = 10/24/16 Pct Recovery = 90% Analysis Date = 10/24/16 Pct Recovery = 90% Analysis Date = 10/23/16 Pct Recovery = 90% Analysis Date = 10/23/16 Pct Recovery = 90% Analysis Date = 10/22/16 Pct Recovery = 91% Analysis Date = 10/22/16 Pct Recovery = 91% Analysis Date = 10/21/16 Pct Recovery = 91% Analysis Date = 10/21/16 Pct Recovery = 91% Analysis Date = 10/20/16 Pct Recovery = 92% Analysis Date = 10/20/16 Pct Recovery = 92% Analysis Date = 10/19/16 Pct Recovery = 92% Analysis Date = 10/19/16 Pct Recovery = 92% Analysis Date = 10/18/16 Pct Recovery = 92% Analysis Date = 10/18/16 Pct Recovery = 92% Analysis Date = 10/17/16 Pct Recovery = 93% Analysis Date = 10/17/16 Pct Recovery = 93% Analysis Date = 10/16/16 Pct Recovery = 93% Analysis Date = 10/16/16 Pct Recovery = 93% Analysis Date = 10/15/16 Pct Recovery = 93% Analysis Date = 10/15/16 Pct Recovery = 93% Analysis Date = 10/14/16 Pct Recovery = 94% Analysis Date = 10/14/16 Pct Recovery = 94% Analysis Date = 10/13/16 Pct Recovery = 94% Analysis Date = 10/13/16 Pct Recovery = 94% Analysis Date = 10/12/16 Pct Recovery = 95% Analysis Date = 10/12/16 Pct Recovery = 95% Analysis Date = 10/11/16 Pct Recovery = 95% Analysis Date = 10/11/16 Pct Recovery = 95% Analysis Date = 10/10/16 Pct Recovery = 95% Analysis Date = 10/10/16 Pct Recovery = 95% Analysis Date = 10/09/16 Pct Recovery = 96% Analysis Date = 10/09/16 Pct Recovery = 96% Analysis Date = 10/08/16 Pct Recovery = 96% Analysis Date = 10/08/16 Pct Recovery = 96% Analysis Date = 10/07/16 Pct Recovery = 96% Analysis Date = 10/07/16 Pct Recovery = 96% Analysis Date = 10/06/16 Pct Recovery = 97% Analysis Date = 10/06/16 Pct Recovery = 97% Analysis Date = 10/05/16 Pct Recovery = 97% Analysis Date = 10/05/16 Pct Recovery = 97% Analysis Date = 10/04/16 Pct Recovery = 98% Analysis Date = 10/04/16 Pct Recovery = 98% Analysis Date = 10/03/16 Pct Recovery = 98% Analysis Date = 10/03/16 Pct Recovery = 98% Analysis Date = 10/02/16 Pct Recovery = 98% Analysis Date = 10/02/16 Pct Recovery = 98% Analysis Date = 10/01/16 Pct Recovery = 99% Analysis Date = 10/01/16 Pct Recovery = 99% Analysis Date = 09/30/16 Pct Recovery = 99% Analysis Date = 09/30/16 Pct Recovery = 99% Analysis Date = 09/29/16 Pct Recovery = 99% Analysis Date = 09/29/16 Pct Recovery = 99% Analysis Date = 09/28/16 Pct Recovery = 100% Analysis Date = 09/28/16 Pct Recovery = 100% Analysis Date = 09/27/16 Pct Recovery = 100% Analysis Date = 09/27/16 Pct Recovery = 100% Analysis Date = 09/26/16 Pct Recovery = 100% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
EQUILENIN

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 4 117% 98% 100% 116%
Total 4 117% 98% 100% 116%

Sample Statistics
EQUILENIN

Characteristic N % % Basis
Plotted 4 36% Spiked
Estimated Values 3 27% Spiked
Deleted Values 2 11% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 12 .  
False Negatives 7 64% 7 out of 11
Not Spiked 7 .  
False Positives 2 33% 2 out of 6

BQS OBSP Determination:
EQUILIN
METHOD: 6434 , TESTIDCODE: 64479GM006
Open Data Set

The SGPlot Procedure

Sample Statistics
EQUILIN

Characteristic N % % Basis
Plotted 0 0% Spiked
Estimated Values 0 0% Spiked
Deleted Values 1 5% Spiked + Not Spiked
Spiked, Censored 1 9% Spiked
Spiked 12 .  
False Negatives 10 91% 10 out of 11
Not Spiked 7 .  
False Positives 0 0% 0 out of 7

BQS OBSP Determination:
ESTRIOL
METHOD: 6434 , TESTIDCODE: 64480GM006
Open Data Set

Analysis Date = 09/26/16 SpikeMix = Abs 051616sed4H3: 0 µl & Abs 051616sed4H2: 0 µl Pct Recovery = 51% Analysis Date = 09/26/16 SpikeMix = Abs 051616sed4H1: 0 µl & Abs 051616sed4L2: 0 µl Pct Recovery = 119% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
ESTRIOL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 2 85% 48% 85% 50%
Total 2 85% 48% 85% 50%

Sample Statistics
ESTRIOL

Characteristic N % % Basis
Plotted 2 20% Spiked
Estimated Values 1 10% Spiked
Deleted Values 2 11% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 12 .  
False Negatives 8 80% 8 out of 10
Not Spiked 7 .  
False Positives 0 0% 0 out of 7

BQS OBSP Determination:
ESTRONE
METHOD: 6434 , TESTIDCODE: 63205GM006
Open Data Set

Analysis Date = 09/26/16 SpikeMix = Abs 051616sed4H1: 0 µl & Abs 051616sed4L2: 0 µl Pct Recovery = 86% Analysis Date = 09/26/16 SpikeMix = Abs 051616sed4H3: 0 µl & Abs 051616sed4H1: 0 µl Pct Recovery = 42% Analysis Date = 05/24/17 SpikeMix = ERA 04121613: 0 µl Pct Recovery = 125% Analysis Date = 04/19/17 SpikeMix = ERA 04121613: 0 µl & ERA 04121614: 0 µl Pct Recovery = 59% Analysis Date = 05/24/17 Pct Recovery = 125% Analysis Date = 05/22/17 Pct Recovery = 122% Analysis Date = 05/22/17 Pct Recovery = 122% Analysis Date = 05/21/17 Pct Recovery = 120% Analysis Date = 05/21/17 Pct Recovery = 120% Analysis Date = 05/20/17 Pct Recovery = 118% Analysis Date = 05/20/17 Pct Recovery = 118% Analysis Date = 05/19/17 Pct Recovery = 116% Analysis Date = 05/19/17 Pct Recovery = 116% Analysis Date = 05/18/17 Pct Recovery = 113% Analysis Date = 05/18/17 Pct Recovery = 113% Analysis Date = 05/16/17 Pct Recovery = 111% Analysis Date = 05/16/17 Pct Recovery = 111% Analysis Date = 05/15/17 Pct Recovery = 109% Analysis Date = 05/15/17 Pct Recovery = 109% Analysis Date = 05/14/17 Pct Recovery = 107% Analysis Date = 05/14/17 Pct Recovery = 107% Analysis Date = 05/13/17 Pct Recovery = 104% Analysis Date = 05/13/17 Pct Recovery = 104% Analysis Date = 05/12/17 Pct Recovery = 102% Analysis Date = 05/12/17 Pct Recovery = 102% Analysis Date = 05/10/17 Pct Recovery = 100% Analysis Date = 05/10/17 Pct Recovery = 100% Analysis Date = 05/09/17 Pct Recovery = 98% Analysis Date = 05/09/17 Pct Recovery = 98% Analysis Date = 05/08/17 Pct Recovery = 95% Analysis Date = 05/08/17 Pct Recovery = 95% Analysis Date = 05/07/17 Pct Recovery = 93% Analysis Date = 05/07/17 Pct Recovery = 93% Analysis Date = 05/06/17 Pct Recovery = 91% Analysis Date = 05/06/17 Pct Recovery = 91% Analysis Date = 05/04/17 Pct Recovery = 89% Analysis Date = 05/04/17 Pct Recovery = 89% Analysis Date = 05/03/17 Pct Recovery = 86% Analysis Date = 05/03/17 Pct Recovery = 86% Analysis Date = 05/02/17 Pct Recovery = 84% Analysis Date = 05/02/17 Pct Recovery = 84% Analysis Date = 05/01/17 Pct Recovery = 82% Analysis Date = 05/01/17 Pct Recovery = 82% Analysis Date = 04/30/17 Pct Recovery = 80% Analysis Date = 04/30/17 Pct Recovery = 80% Analysis Date = 04/28/17 Pct Recovery = 78% Analysis Date = 04/28/17 Pct Recovery = 78% Analysis Date = 04/27/17 Pct Recovery = 75% Analysis Date = 04/27/17 Pct Recovery = 75% Analysis Date = 04/26/17 Pct Recovery = 73% Analysis Date = 04/26/17 Pct Recovery = 73% Analysis Date = 04/25/17 Pct Recovery = 71% Analysis Date = 04/25/17 Pct Recovery = 71% Analysis Date = 04/24/17 Pct Recovery = 69% Analysis Date = 04/24/17 Pct Recovery = 69% Analysis Date = 04/22/17 Pct Recovery = 66% Analysis Date = 04/22/17 Pct Recovery = 66% Analysis Date = 04/21/17 Pct Recovery = 64% Analysis Date = 04/21/17 Pct Recovery = 64% Analysis Date = 04/20/17 Pct Recovery = 62% Analysis Date = 04/20/17 Pct Recovery = 62% Analysis Date = 04/19/17 Pct Recovery = 60% Analysis Date = 04/19/17 Pct Recovery = 60% Analysis Date = 04/18/17 Pct Recovery = 59% Analysis Date = 04/18/17 Pct Recovery = 59% Analysis Date = 04/16/17 Pct Recovery = 59% Analysis Date = 04/16/17 Pct Recovery = 59% Analysis Date = 04/15/17 Pct Recovery = 59% Analysis Date = 04/15/17 Pct Recovery = 59% Analysis Date = 04/14/17 Pct Recovery = 59% Analysis Date = 04/14/17 Pct Recovery = 59% Analysis Date = 04/13/17 Pct Recovery = 59% Analysis Date = 04/13/17 Pct Recovery = 59% Analysis Date = 04/12/17 Pct Recovery = 59% Analysis Date = 04/12/17 Pct Recovery = 59% Analysis Date = 04/10/17 Pct Recovery = 59% Analysis Date = 04/10/17 Pct Recovery = 59% Analysis Date = 04/09/17 Pct Recovery = 60% Analysis Date = 04/09/17 Pct Recovery = 60% Analysis Date = 04/08/17 Pct Recovery = 60% Analysis Date = 04/08/17 Pct Recovery = 60% Analysis Date = 04/07/17 Pct Recovery = 60% Analysis Date = 04/07/17 Pct Recovery = 60% Analysis Date = 04/06/17 Pct Recovery = 60% Analysis Date = 04/06/17 Pct Recovery = 60% Analysis Date = 04/04/17 Pct Recovery = 60% Analysis Date = 04/04/17 Pct Recovery = 60% Analysis Date = 04/03/17 Pct Recovery = 60% Analysis Date = 04/03/17 Pct Recovery = 60% Analysis Date = 04/02/17 Pct Recovery = 60% Analysis Date = 04/02/17 Pct Recovery = 60% Analysis Date = 04/01/17 Pct Recovery = 60% Analysis Date = 04/01/17 Pct Recovery = 60% Analysis Date = 03/31/17 Pct Recovery = 60% Analysis Date = 03/31/17 Pct Recovery = 60% Analysis Date = 03/29/17 Pct Recovery = 60% Analysis Date = 03/29/17 Pct Recovery = 60% Analysis Date = 03/28/17 Pct Recovery = 60% Analysis Date = 03/28/17 Pct Recovery = 60% Analysis Date = 03/27/17 Pct Recovery = 60% Analysis Date = 03/27/17 Pct Recovery = 60% Analysis Date = 03/26/17 Pct Recovery = 60% Analysis Date = 03/26/17 Pct Recovery = 60% Analysis Date = 03/25/17 Pct Recovery = 60% Analysis Date = 03/25/17 Pct Recovery = 60% Analysis Date = 03/23/17 Pct Recovery = 60% Analysis Date = 03/23/17 Pct Recovery = 60% Analysis Date = 03/22/17 Pct Recovery = 60% Analysis Date = 03/22/17 Pct Recovery = 60% Analysis Date = 03/21/17 Pct Recovery = 60% Analysis Date = 03/21/17 Pct Recovery = 60% Analysis Date = 03/20/17 Pct Recovery = 60% Analysis Date = 03/20/17 Pct Recovery = 60% Analysis Date = 03/19/17 Pct Recovery = 60% Analysis Date = 03/19/17 Pct Recovery = 60% Analysis Date = 03/17/17 Pct Recovery = 60% Analysis Date = 03/17/17 Pct Recovery = 60% Analysis Date = 03/16/17 Pct Recovery = 60% Analysis Date = 03/16/17 Pct Recovery = 60% Analysis Date = 03/15/17 Pct Recovery = 60% Analysis Date = 03/15/17 Pct Recovery = 60% Analysis Date = 03/14/17 Pct Recovery = 60% Analysis Date = 03/14/17 Pct Recovery = 60% Analysis Date = 03/13/17 Pct Recovery = 60% Analysis Date = 03/13/17 Pct Recovery = 60% Analysis Date = 03/11/17 Pct Recovery = 60% Analysis Date = 03/11/17 Pct Recovery = 60% Analysis Date = 03/10/17 Pct Recovery = 60% Analysis Date = 03/10/17 Pct Recovery = 60% Analysis Date = 03/09/17 Pct Recovery = 60% Analysis Date = 03/09/17 Pct Recovery = 60% Analysis Date = 03/08/17 Pct Recovery = 60% Analysis Date = 03/08/17 Pct Recovery = 60% Analysis Date = 03/07/17 Pct Recovery = 60% Analysis Date = 03/07/17 Pct Recovery = 60% Analysis Date = 03/05/17 Pct Recovery = 60% Analysis Date = 03/05/17 Pct Recovery = 60% Analysis Date = 03/04/17 Pct Recovery = 60% Analysis Date = 03/04/17 Pct Recovery = 60% Analysis Date = 03/03/17 Pct Recovery = 60% Analysis Date = 03/03/17 Pct Recovery = 60% Analysis Date = 03/02/17 Pct Recovery = 60% Analysis Date = 03/02/17 Pct Recovery = 60% Analysis Date = 03/01/17 Pct Recovery = 60% Analysis Date = 03/01/17 Pct Recovery = 60% Analysis Date = 02/27/17 Pct Recovery = 60% Analysis Date = 02/27/17 Pct Recovery = 60% Analysis Date = 02/26/17 Pct Recovery = 61% Analysis Date = 02/26/17 Pct Recovery = 61% Analysis Date = 02/25/17 Pct Recovery = 61% Analysis Date = 02/25/17 Pct Recovery = 61% Analysis Date = 02/24/17 Pct Recovery = 61% Analysis Date = 02/24/17 Pct Recovery = 61% Analysis Date = 02/23/17 Pct Recovery = 61% Analysis Date = 02/23/17 Pct Recovery = 61% Analysis Date = 02/21/17 Pct Recovery = 61% Analysis Date = 02/21/17 Pct Recovery = 61% Analysis Date = 02/20/17 Pct Recovery = 61% Analysis Date = 02/20/17 Pct Recovery = 61% Analysis Date = 02/19/17 Pct Recovery = 61% Analysis Date = 02/19/17 Pct Recovery = 61% Analysis Date = 02/18/17 Pct Recovery = 61% Analysis Date = 02/18/17 Pct Recovery = 61% Analysis Date = 02/17/17 Pct Recovery = 61% Analysis Date = 02/17/17 Pct Recovery = 61% Analysis Date = 02/15/17 Pct Recovery = 61% Analysis Date = 02/15/17 Pct Recovery = 61% Analysis Date = 02/14/17 Pct Recovery = 61% Analysis Date = 02/14/17 Pct Recovery = 61% Analysis Date = 02/13/17 Pct Recovery = 61% Analysis Date = 02/13/17 Pct Recovery = 61% Analysis Date = 02/12/17 Pct Recovery = 61% Analysis Date = 02/12/17 Pct Recovery = 61% Analysis Date = 02/11/17 Pct Recovery = 61% Analysis Date = 02/11/17 Pct Recovery = 61% Analysis Date = 02/09/17 Pct Recovery = 61% Analysis Date = 02/09/17 Pct Recovery = 61% Analysis Date = 02/08/17 Pct Recovery = 61% Analysis Date = 02/08/17 Pct Recovery = 61% Analysis Date = 02/07/17 Pct Recovery = 61% Analysis Date = 02/07/17 Pct Recovery = 61% Analysis Date = 02/06/17 Pct Recovery = 61% Analysis Date = 02/06/17 Pct Recovery = 61% Analysis Date = 02/05/17 Pct Recovery = 61% Analysis Date = 02/05/17 Pct Recovery = 61% Analysis Date = 02/03/17 Pct Recovery = 61% Analysis Date = 02/03/17 Pct Recovery = 61% Analysis Date = 02/02/17 Pct Recovery = 61% Analysis Date = 02/02/17 Pct Recovery = 61% Analysis Date = 02/01/17 Pct Recovery = 61% Analysis Date = 02/01/17 Pct Recovery = 61% Analysis Date = 01/31/17 Pct Recovery = 61% Analysis Date = 01/31/17 Pct Recovery = 61% Analysis Date = 01/30/17 Pct Recovery = 61% Analysis Date = 01/30/17 Pct Recovery = 61% Analysis Date = 01/28/17 Pct Recovery = 61% Analysis Date = 01/28/17 Pct Recovery = 61% Analysis Date = 01/27/17 Pct Recovery = 61% Analysis Date = 01/27/17 Pct Recovery = 61% Analysis Date = 01/26/17 Pct Recovery = 61% Analysis Date = 01/26/17 Pct Recovery = 61% Analysis Date = 01/25/17 Pct Recovery = 61% Analysis Date = 01/25/17 Pct Recovery = 61% Analysis Date = 01/24/17 Pct Recovery = 61% Analysis Date = 01/24/17 Pct Recovery = 61% Analysis Date = 01/22/17 Pct Recovery = 61% Analysis Date = 01/22/17 Pct Recovery = 61% Analysis Date = 01/21/17 Pct Recovery = 61% Analysis Date = 01/21/17 Pct Recovery = 61% Analysis Date = 01/20/17 Pct Recovery = 61% Analysis Date = 01/20/17 Pct Recovery = 61% Analysis Date = 01/19/17 Pct Recovery = 61% Analysis Date = 01/19/17 Pct Recovery = 61% Analysis Date = 01/18/17 Pct Recovery = 61% Analysis Date = 01/18/17 Pct Recovery = 61% Analysis Date = 01/16/17 Pct Recovery = 61% Analysis Date = 01/16/17 Pct Recovery = 61% Analysis Date = 01/15/17 Pct Recovery = 62% Analysis Date = 01/15/17 Pct Recovery = 62% Analysis Date = 01/14/17 Pct Recovery = 62% Analysis Date = 01/14/17 Pct Recovery = 62% Analysis Date = 01/13/17 Pct Recovery = 62% Analysis Date = 01/13/17 Pct Recovery = 62% Analysis Date = 01/12/17 Pct Recovery = 62% Analysis Date = 01/12/17 Pct Recovery = 62% Analysis Date = 01/10/17 Pct Recovery = 62% Analysis Date = 01/10/17 Pct Recovery = 62% Analysis Date = 01/09/17 Pct Recovery = 62% Analysis Date = 01/09/17 Pct Recovery = 62% Analysis Date = 01/08/17 Pct Recovery = 62% Analysis Date = 01/08/17 Pct Recovery = 62% Analysis Date = 01/07/17 Pct Recovery = 62% Analysis Date = 01/07/17 Pct Recovery = 62% Analysis Date = 01/06/17 Pct Recovery = 62% Analysis Date = 01/06/17 Pct Recovery = 62% Analysis Date = 01/04/17 Pct Recovery = 62% Analysis Date = 01/04/17 Pct Recovery = 62% Analysis Date = 01/03/17 Pct Recovery = 62% Analysis Date = 01/03/17 Pct Recovery = 62% Analysis Date = 01/02/17 Pct Recovery = 62% Analysis Date = 01/02/17 Pct Recovery = 62% Analysis Date = 01/01/17 Pct Recovery = 62% Analysis Date = 01/01/17 Pct Recovery = 62% Analysis Date = 12/31/16 Pct Recovery = 62% Analysis Date = 12/31/16 Pct Recovery = 62% Analysis Date = 12/29/16 Pct Recovery = 62% Analysis Date = 12/29/16 Pct Recovery = 62% Analysis Date = 12/28/16 Pct Recovery = 62% Analysis Date = 12/28/16 Pct Recovery = 62% Analysis Date = 12/27/16 Pct Recovery = 62% Analysis Date = 12/27/16 Pct Recovery = 62% Analysis Date = 12/26/16 Pct Recovery = 62% Analysis Date = 12/26/16 Pct Recovery = 62% Analysis Date = 12/25/16 Pct Recovery = 62% Analysis Date = 12/25/16 Pct Recovery = 62% Analysis Date = 12/23/16 Pct Recovery = 62% Analysis Date = 12/23/16 Pct Recovery = 62% Analysis Date = 12/22/16 Pct Recovery = 62% Analysis Date = 12/22/16 Pct Recovery = 62% Analysis Date = 12/21/16 Pct Recovery = 62% Analysis Date = 12/21/16 Pct Recovery = 62% Analysis Date = 12/20/16 Pct Recovery = 62% Analysis Date = 12/20/16 Pct Recovery = 62% Analysis Date = 12/19/16 Pct Recovery = 62% Analysis Date = 12/19/16 Pct Recovery = 62% Analysis Date = 12/17/16 Pct Recovery = 62% Analysis Date = 12/17/16 Pct Recovery = 62% Analysis Date = 12/16/16 Pct Recovery = 62% Analysis Date = 12/16/16 Pct Recovery = 62% Analysis Date = 12/15/16 Pct Recovery = 62% Analysis Date = 12/15/16 Pct Recovery = 62% Analysis Date = 12/14/16 Pct Recovery = 62% Analysis Date = 12/14/16 Pct Recovery = 62% Analysis Date = 12/13/16 Pct Recovery = 62% Analysis Date = 12/13/16 Pct Recovery = 62% Analysis Date = 12/11/16 Pct Recovery = 62% Analysis Date = 12/11/16 Pct Recovery = 62% Analysis Date = 12/10/16 Pct Recovery = 62% Analysis Date = 12/10/16 Pct Recovery = 62% Analysis Date = 12/09/16 Pct Recovery = 62% Analysis Date = 12/09/16 Pct Recovery = 62% Analysis Date = 12/08/16 Pct Recovery = 62% Analysis Date = 12/08/16 Pct Recovery = 62% Analysis Date = 12/07/16 Pct Recovery = 62% Analysis Date = 12/07/16 Pct Recovery = 62% Analysis Date = 12/05/16 Pct Recovery = 63% Analysis Date = 12/05/16 Pct Recovery = 63% Analysis Date = 12/04/16 Pct Recovery = 63% Analysis Date = 12/04/16 Pct Recovery = 63% Analysis Date = 12/03/16 Pct Recovery = 63% Analysis Date = 12/03/16 Pct Recovery = 63% Analysis Date = 12/02/16 Pct Recovery = 63% Analysis Date = 12/02/16 Pct Recovery = 63% Analysis Date = 12/01/16 Pct Recovery = 63% Analysis Date = 12/01/16 Pct Recovery = 63% Analysis Date = 11/29/16 Pct Recovery = 63% Analysis Date = 11/29/16 Pct Recovery = 63% Analysis Date = 11/28/16 Pct Recovery = 63% Analysis Date = 11/28/16 Pct Recovery = 63% Analysis Date = 11/27/16 Pct Recovery = 63% Analysis Date = 11/27/16 Pct Recovery = 63% Analysis Date = 11/26/16 Pct Recovery = 63% Analysis Date = 11/26/16 Pct Recovery = 63% Analysis Date = 11/25/16 Pct Recovery = 63% Analysis Date = 11/25/16 Pct Recovery = 63% Analysis Date = 11/23/16 Pct Recovery = 63% Analysis Date = 11/23/16 Pct Recovery = 63% Analysis Date = 11/22/16 Pct Recovery = 63% Analysis Date = 11/22/16 Pct Recovery = 63% Analysis Date = 11/21/16 Pct Recovery = 63% Analysis Date = 11/21/16 Pct Recovery = 63% Analysis Date = 11/20/16 Pct Recovery = 63% Analysis Date = 11/20/16 Pct Recovery = 63% Analysis Date = 11/19/16 Pct Recovery = 63% Analysis Date = 11/19/16 Pct Recovery = 63% Analysis Date = 11/17/16 Pct Recovery = 63% Analysis Date = 11/17/16 Pct Recovery = 63% Analysis Date = 11/16/16 Pct Recovery = 63% Analysis Date = 11/16/16 Pct Recovery = 63% Analysis Date = 11/15/16 Pct Recovery = 63% Analysis Date = 11/15/16 Pct Recovery = 63% Analysis Date = 11/14/16 Pct Recovery = 63% Analysis Date = 11/14/16 Pct Recovery = 63% Analysis Date = 11/13/16 Pct Recovery = 63% Analysis Date = 11/13/16 Pct Recovery = 63% Analysis Date = 11/11/16 Pct Recovery = 63% Analysis Date = 11/11/16 Pct Recovery = 63% Analysis Date = 11/10/16 Pct Recovery = 63% Analysis Date = 11/10/16 Pct Recovery = 63% Analysis Date = 11/09/16 Pct Recovery = 63% Analysis Date = 11/09/16 Pct Recovery = 63% Analysis Date = 11/08/16 Pct Recovery = 63% Analysis Date = 11/08/16 Pct Recovery = 63% Analysis Date = 11/07/16 Pct Recovery = 63% Analysis Date = 11/07/16 Pct Recovery = 63% Analysis Date = 11/05/16 Pct Recovery = 63% Analysis Date = 11/05/16 Pct Recovery = 63% Analysis Date = 11/04/16 Pct Recovery = 63% Analysis Date = 11/04/16 Pct Recovery = 63% Analysis Date = 11/03/16 Pct Recovery = 63% Analysis Date = 11/03/16 Pct Recovery = 63% Analysis Date = 11/02/16 Pct Recovery = 63% Analysis Date = 11/02/16 Pct Recovery = 63% Analysis Date = 11/01/16 Pct Recovery = 63% Analysis Date = 11/01/16 Pct Recovery = 63% Analysis Date = 10/30/16 Pct Recovery = 63% Analysis Date = 10/30/16 Pct Recovery = 63% Analysis Date = 10/29/16 Pct Recovery = 63% Analysis Date = 10/29/16 Pct Recovery = 63% Analysis Date = 10/28/16 Pct Recovery = 63% Analysis Date = 10/28/16 Pct Recovery = 63% Analysis Date = 10/27/16 Pct Recovery = 63% Analysis Date = 10/27/16 Pct Recovery = 63% Analysis Date = 10/26/16 Pct Recovery = 63% Analysis Date = 10/26/16 Pct Recovery = 63% Analysis Date = 10/24/16 Pct Recovery = 64% Analysis Date = 10/24/16 Pct Recovery = 64% Analysis Date = 10/23/16 Pct Recovery = 64% Analysis Date = 10/23/16 Pct Recovery = 64% Analysis Date = 10/22/16 Pct Recovery = 64% Analysis Date = 10/22/16 Pct Recovery = 64% Analysis Date = 10/21/16 Pct Recovery = 64% Analysis Date = 10/21/16 Pct Recovery = 64% Analysis Date = 10/20/16 Pct Recovery = 64% Analysis Date = 10/20/16 Pct Recovery = 64% Analysis Date = 10/18/16 Pct Recovery = 64% Analysis Date = 10/18/16 Pct Recovery = 64% Analysis Date = 10/17/16 Pct Recovery = 64% Analysis Date = 10/17/16 Pct Recovery = 64% Analysis Date = 10/16/16 Pct Recovery = 64% Analysis Date = 10/16/16 Pct Recovery = 64% Analysis Date = 10/15/16 Pct Recovery = 64% Analysis Date = 10/15/16 Pct Recovery = 64% Analysis Date = 10/14/16 Pct Recovery = 64% Analysis Date = 10/14/16 Pct Recovery = 64% Analysis Date = 10/12/16 Pct Recovery = 64% Analysis Date = 10/12/16 Pct Recovery = 64% Analysis Date = 10/11/16 Pct Recovery = 64% Analysis Date = 10/11/16 Pct Recovery = 64% Analysis Date = 10/10/16 Pct Recovery = 64% Analysis Date = 10/10/16 Pct Recovery = 64% Analysis Date = 10/09/16 Pct Recovery = 64% Analysis Date = 10/09/16 Pct Recovery = 64% Analysis Date = 10/08/16 Pct Recovery = 64% Analysis Date = 10/08/16 Pct Recovery = 64% Analysis Date = 10/06/16 Pct Recovery = 64% Analysis Date = 10/06/16 Pct Recovery = 64% Analysis Date = 10/05/16 Pct Recovery = 64% Analysis Date = 10/05/16 Pct Recovery = 64% Analysis Date = 10/04/16 Pct Recovery = 64% Analysis Date = 10/04/16 Pct Recovery = 64% Analysis Date = 10/03/16 Pct Recovery = 64% Analysis Date = 10/03/16 Pct Recovery = 64% Analysis Date = 10/02/16 Pct Recovery = 64% Analysis Date = 10/02/16 Pct Recovery = 64% Analysis Date = 09/30/16 Pct Recovery = 64% Analysis Date = 09/30/16 Pct Recovery = 64% Analysis Date = 09/29/16 Pct Recovery = 64% Analysis Date = 09/29/16 Pct Recovery = 64% Analysis Date = 09/28/16 Pct Recovery = 64% Analysis Date = 09/28/16 Pct Recovery = 64% Analysis Date = 09/27/16 Pct Recovery = 64% Analysis Date = 09/27/16 Pct Recovery = 64% Analysis Date = 09/26/16 Pct Recovery = 64% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
ESTRONE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 4 78% 36% 73% 41%
Total 4 78% 36% 73% 41%

Sample Statistics
ESTRONE

Characteristic N % % Basis
Plotted 4 33% Spiked
Estimated Values 0 0% Spiked
Deleted Values 1 5% Spiked + Not Spiked
Spiked, Censored 2 17% Spiked
Spiked 12 .  
False Negatives 6 50% 6 out of 12
Not Spiked 7 .  
False Positives 0 0% 0 out of 6

BQS OBSP Determination:
MESTRANOL
METHOD: 6434 , TESTIDCODE: 63638GM006
Open Data Set

Analysis Date = 09/26/16 SpikeMix = Abs 051616sed4H3: 0 µl & Abs 051616sed4H2: 0 µl Pct Recovery = 60% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
MESTRANOL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 1 60% . 60% 0%
Total 1 60% . 60% 0%

Sample Statistics
MESTRANOL

Characteristic N % % Basis
Plotted 1 9% Spiked
Estimated Values 0 0% Spiked
Deleted Values 1 5% Spiked + Not Spiked
Spiked, Censored 1 9% Spiked
Spiked 12 .  
False Negatives 9 82% 9 out of 11
Not Spiked 7 .  
False Positives 0 0% 0 out of 7

BQS OBSP Determination:
NORETHINDRONE
METHOD: 6434 , TESTIDCODE: 63644GM006
Open Data Set

Analysis Date = 09/26/16 SpikeMix = Abs 051616sed4H3: 0 µl & Abs 051616sed4H1: 0 µl Pct Recovery = 33% Analysis Date = 05/24/17 SpikeMix = ERA 04121615: 0 µl Pct Recovery = 123% Analysis Date = 03/17/17 SpikeMix = ERA 04121614: 0 µl & ERA 04121615: 0 µl Pct Recovery = 60% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
NORETHINDRONE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 3 72% 46% 60% 67%
Total 3 72% 46% 60% 67%

Sample Statistics
NORETHINDRONE

Characteristic N % % Basis
Plotted 3 27% Spiked
Estimated Values 0 0% Spiked
Deleted Values 1 5% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 12 .  
False Negatives 8 73% 8 out of 11
Not Spiked 7 .  
False Positives 0 0% 0 out of 7

BQS OBSP Determination:
PROGESTERONE
METHOD: 6434 , TESTIDCODE: 63657GM006
Open Data Set

The SGPlot Procedure

Sample Statistics
PROGESTERONE

Characteristic N % % Basis
Plotted 0 0% Spiked
Estimated Values 0 0% Spiked
Deleted Values 5 26% Spiked + Not Spiked
Spiked, Censored 7 88% Spiked
Spiked 12 .  
False Negatives 1 13% 1 out of 8
Not Spiked 7 .  
False Positives 1 17% 1 out of 6

BQS OBSP Determination:
TESTOSTERONE
METHOD: 6434 , TESTIDCODE: 64485GM006
Open Data Set

Analysis Date = 09/26/16 SpikeMix = Abs 051616sed4H1: 0 µl & Abs 051616sed4L2: 0 µl Pct Recovery = 194% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
TESTOSTERONE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 1 194% . 194% 0%
Total 1 194% . 194% 0%

Sample Statistics
TESTOSTERONE

Characteristic N % % Basis
Plotted 1 20% Spiked
Estimated Values 1 20% Spiked
Deleted Values 1 5% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 6 .  
False Negatives 4 80% 4 out of 5
Not Spiked 13 .  
False Positives 1 8% 1 out of 13

BQS OBSP Determination:
TRANS-DIETHYLSTILBESTROL
METHOD: 6434 , TESTIDCODE: 63620GM006
Open Data Set

The SGPlot Procedure

Sample Statistics
TRANS-DIETHYLSTILBESTROL

Characteristic N % % Basis
Plotted 0 0% Spiked
Estimated Values 0 0% Spiked
Deleted Values 10 53% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 12 .  
False Negatives 6 100% 6 out of 6
Not Spiked 7 .  
False Positives 0 0% 0 out of 3