BQS OBSP Determination:
1,1,1,2-TETRACHLOROETHANE
METHOD: 4440 , TESTIDCODE: 77562GCM66
Open Data Set

Analysis Date = 12/16/16 SpikeMix = NSI 041816AVOC: 40 µl & ChemService 5082900: 40 µl Pct Recovery = 96% Analysis Date = 08/04/16 SpikeMix = Crescent 03FF058: 40 µl & Supelco LC20141V: 40 µl Pct Recovery = 88% Analysis Date = 07/20/16 SpikeMix = Supelco LC20141V: 40 µl & Accu 216041125: 40 µl Pct Recovery = 91% Analysis Date = 08/26/16 SpikeMix = NSI 041816AVOC: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 99% Analysis Date = 08/12/16 SpikeMix = ChemService 5082900: 25 µl & Phenova B20160319: 25 µl Pct Recovery = 90% Analysis Date = 06/30/16 SpikeMix = Crescent 03FF058: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 104% Analysis Date = 11/21/16 SpikeMix = Crescent 03FF058: 25 µl & Supelco LC20141V: 25 µl Pct Recovery = 93% Analysis Date = 09/08/16 SpikeMix = Supelco LC20141V: 25 µl & Accu 216041125: 25 µl Pct Recovery = 91% Analysis Date = 04/09/15 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 99% Analysis Date = 03/06/15 SpikeMix = ERA 0227-14-06.1A: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 95% Analysis Date = 11/14/14 SpikeMix = Crescent 03DD004: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 88% Analysis Date = 08/16/14 SpikeMix = ERA 0227-14-06.1A: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 98% Analysis Date = 07/01/14 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 100% Analysis Date = 11/22/14 SpikeMix = NSI 032614: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 92% Analysis Date = 06/10/14 SpikeMix = Crescent 03DD004: 20 µl & NSI 032614: 20 µl Pct Recovery = 91% Analysis Date = 06/10/14 SpikeMix = NSI 032614: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 95% Analysis Date = 05/01/14 SpikeMix = Accu 214031115: 20 µl & NSI 032614: 20 µl Pct Recovery = 91% Analysis Date = 08/15/15 SpikeMix = Supelco LC13545: 25 µl & Crescent 04EE008: 25 µl Pct Recovery = 101% Analysis Date = 07/13/15 SpikeMix = Crescent 04EE008: 25 µl & NSI 050515AVOC: 25 µl Pct Recovery = 91% Analysis Date = 09/29/15 SpikeMix = Accu 215041380: 25 µl & ERA 0406-15-03: 25 µl Pct Recovery = 89% Analysis Date = 11/29/16 SpikeMix = ChemService 5082900: 15 µl & Phenova B20160319: 15 µl Pct Recovery = 99% Analysis Date = 09/28/16 SpikeMix = Crescent 03FF058: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 105% Analysis Date = 06/30/16 SpikeMix = ChemService 5082900: 15 µl & Accu 216041125: 15 µl Pct Recovery = 105% Analysis Date = 06/10/16 SpikeMix = NSI 041816AVOC: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 87% Analysis Date = 10/13/16 SpikeMix = NSI 041816AVOC: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 98% Analysis Date = 05/27/16 SpikeMix = Phenova B20160319: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 98% Analysis Date = 12/18/15 SpikeMix = Supelco LC13545: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 87% Analysis Date = 10/17/15 SpikeMix = Crescent 04EE008: 15 µl & NSI 050515AVOC: 15 µl Pct Recovery = 84% Analysis Date = 05/09/15 SpikeMix = Spex Organics EN150428007: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 91% Analysis Date = 04/02/16 SpikeMix = Supelco LC13545: 15 µl & Accu 215041380: 15 µl Pct Recovery = 88% Analysis Date = 03/04/16 SpikeMix = Accu 215041380: 15 µl & ERA 0406-15-03: 15 µl Pct Recovery = 90% Analysis Date = 06/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Accu 215041380: 15 µl Pct Recovery = 87% Analysis Date = 01/13/15 SpikeMix = Accu 214031115: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 90% Analysis Date = 10/21/14 SpikeMix = ERA 0227-14-06.1A: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 91% Analysis Date = 10/04/14 SpikeMix = Crescent 03DD004: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 101% Analysis Date = 07/11/14 SpikeMix = Spex Organics C1140417015: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 93% Analysis Date = 09/09/14 SpikeMix = Accu 214031115: 10 µl & NSI 032614: 10 µl Pct Recovery = 99% Analysis Date = 09/09/14 SpikeMix = NSI 032614: 10 µl & Spex Organics C1140417015: 10 µl Pct Recovery = 100% Analysis Date = 07/29/14 SpikeMix = Crescent 03DD004: 10 µl & NSI 032614: 10 µl Pct Recovery = 109% Analysis Date = 05/30/14 SpikeMix = NSI 032614: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 94% Analysis Date = 05/13/16 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 105% Analysis Date = 01/27/16 SpikeMix = Crescent 04EE008: 10 µl & NSI 050515AVOC: 10 µl Pct Recovery = 97% Analysis Date = 08/07/15 SpikeMix = Crescent 04EE008: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 90% Analysis Date = 05/09/15 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 88% Analysis Date = 02/18/16 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 88% Analysis Date = 11/20/15 SpikeMix = Accu 215041380: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 90% Analysis Date = 11/12/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 90% Analysis Date = 05/21/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 85% Analysis Date = 12/15/16 Pct Recovery = 98% Analysis Date = 12/11/16 Pct Recovery = 98% Analysis Date = 12/11/16 Pct Recovery = 98% Analysis Date = 12/06/16 Pct Recovery = 98% Analysis Date = 12/06/16 Pct Recovery = 98% Analysis Date = 12/01/16 Pct Recovery = 98% Analysis Date = 12/01/16 Pct Recovery = 98% Analysis Date = 11/26/16 Pct Recovery = 98% Analysis Date = 11/26/16 Pct Recovery = 98% Analysis Date = 11/21/16 Pct Recovery = 98% Analysis Date = 11/21/16 Pct Recovery = 98% Analysis Date = 11/17/16 Pct Recovery = 97% Analysis Date = 11/17/16 Pct Recovery = 97% Analysis Date = 11/12/16 Pct Recovery = 97% Analysis Date = 11/12/16 Pct Recovery = 97% Analysis Date = 11/07/16 Pct Recovery = 97% Analysis Date = 11/07/16 Pct Recovery = 97% Analysis Date = 11/02/16 Pct Recovery = 97% Analysis Date = 11/02/16 Pct Recovery = 97% Analysis Date = 10/28/16 Pct Recovery = 97% Analysis Date = 10/28/16 Pct Recovery = 97% Analysis Date = 10/24/16 Pct Recovery = 97% Analysis Date = 10/24/16 Pct Recovery = 97% Analysis Date = 10/19/16 Pct Recovery = 97% Analysis Date = 10/19/16 Pct Recovery = 97% Analysis Date = 10/14/16 Pct Recovery = 97% Analysis Date = 10/14/16 Pct Recovery = 97% Analysis Date = 10/09/16 Pct Recovery = 97% Analysis Date = 10/09/16 Pct Recovery = 97% Analysis Date = 10/04/16 Pct Recovery = 97% Analysis Date = 10/04/16 Pct Recovery = 97% Analysis Date = 09/30/16 Pct Recovery = 97% Analysis Date = 09/30/16 Pct Recovery = 97% Analysis Date = 09/25/16 Pct Recovery = 97% Analysis Date = 09/25/16 Pct Recovery = 97% Analysis Date = 09/20/16 Pct Recovery = 96% Analysis Date = 09/20/16 Pct Recovery = 96% Analysis Date = 09/15/16 Pct Recovery = 96% Analysis Date = 09/15/16 Pct Recovery = 96% Analysis Date = 09/10/16 Pct Recovery = 96% Analysis Date = 09/10/16 Pct Recovery = 96% Analysis Date = 09/06/16 Pct Recovery = 96% Analysis Date = 09/06/16 Pct Recovery = 96% Analysis Date = 09/01/16 Pct Recovery = 96% Analysis Date = 09/01/16 Pct Recovery = 96% Analysis Date = 08/27/16 Pct Recovery = 96% Analysis Date = 08/27/16 Pct Recovery = 96% Analysis Date = 08/22/16 Pct Recovery = 96% Analysis Date = 08/22/16 Pct Recovery = 96% Analysis Date = 08/17/16 Pct Recovery = 96% Analysis Date = 08/17/16 Pct Recovery = 96% Analysis Date = 08/13/16 Pct Recovery = 96% Analysis Date = 08/13/16 Pct Recovery = 96% Analysis Date = 08/08/16 Pct Recovery = 96% Analysis Date = 08/08/16 Pct Recovery = 96% Analysis Date = 08/03/16 Pct Recovery = 96% Analysis Date = 08/03/16 Pct Recovery = 96% Analysis Date = 07/29/16 Pct Recovery = 95% Analysis Date = 07/29/16 Pct Recovery = 95% Analysis Date = 07/24/16 Pct Recovery = 95% Analysis Date = 07/24/16 Pct Recovery = 95% Analysis Date = 07/20/16 Pct Recovery = 95% Analysis Date = 07/20/16 Pct Recovery = 95% Analysis Date = 07/15/16 Pct Recovery = 95% Analysis Date = 07/15/16 Pct Recovery = 95% Analysis Date = 07/10/16 Pct Recovery = 95% Analysis Date = 07/10/16 Pct Recovery = 95% Analysis Date = 07/05/16 Pct Recovery = 95% Analysis Date = 07/05/16 Pct Recovery = 95% Analysis Date = 06/30/16 Pct Recovery = 95% Analysis Date = 06/30/16 Pct Recovery = 95% Analysis Date = 06/26/16 Pct Recovery = 95% Analysis Date = 06/26/16 Pct Recovery = 95% Analysis Date = 06/21/16 Pct Recovery = 95% Analysis Date = 06/21/16 Pct Recovery = 95% Analysis Date = 06/16/16 Pct Recovery = 95% Analysis Date = 06/16/16 Pct Recovery = 95% Analysis Date = 06/11/16 Pct Recovery = 94% Analysis Date = 06/11/16 Pct Recovery = 94% Analysis Date = 06/06/16 Pct Recovery = 94% Analysis Date = 06/06/16 Pct Recovery = 94% Analysis Date = 06/02/16 Pct Recovery = 94% Analysis Date = 06/02/16 Pct Recovery = 94% Analysis Date = 05/28/16 Pct Recovery = 94% Analysis Date = 05/28/16 Pct Recovery = 94% Analysis Date = 05/23/16 Pct Recovery = 94% Analysis Date = 05/23/16 Pct Recovery = 94% Analysis Date = 05/18/16 Pct Recovery = 94% Analysis Date = 05/18/16 Pct Recovery = 94% Analysis Date = 05/13/16 Pct Recovery = 94% Analysis Date = 05/13/16 Pct Recovery = 94% Analysis Date = 05/09/16 Pct Recovery = 94% Analysis Date = 05/09/16 Pct Recovery = 94% Analysis Date = 05/04/16 Pct Recovery = 94% Analysis Date = 05/04/16 Pct Recovery = 94% Analysis Date = 04/29/16 Pct Recovery = 94% Analysis Date = 04/29/16 Pct Recovery = 94% Analysis Date = 04/24/16 Pct Recovery = 94% Analysis Date = 04/24/16 Pct Recovery = 94% Analysis Date = 04/19/16 Pct Recovery = 93% Analysis Date = 04/19/16 Pct Recovery = 93% Analysis Date = 04/15/16 Pct Recovery = 93% Analysis Date = 04/15/16 Pct Recovery = 93% Analysis Date = 04/10/16 Pct Recovery = 93% Analysis Date = 04/10/16 Pct Recovery = 93% Analysis Date = 04/05/16 Pct Recovery = 93% Analysis Date = 04/05/16 Pct Recovery = 93% Analysis Date = 03/31/16 Pct Recovery = 93% Analysis Date = 03/31/16 Pct Recovery = 93% Analysis Date = 03/26/16 Pct Recovery = 93% Analysis Date = 03/26/16 Pct Recovery = 93% Analysis Date = 03/22/16 Pct Recovery = 93% Analysis Date = 03/22/16 Pct Recovery = 93% Analysis Date = 03/17/16 Pct Recovery = 93% Analysis Date = 03/17/16 Pct Recovery = 93% Analysis Date = 03/12/16 Pct Recovery = 93% Analysis Date = 03/12/16 Pct Recovery = 93% Analysis Date = 03/07/16 Pct Recovery = 93% Analysis Date = 03/07/16 Pct Recovery = 93% Analysis Date = 03/02/16 Pct Recovery = 92% Analysis Date = 03/02/16 Pct Recovery = 92% Analysis Date = 02/27/16 Pct Recovery = 92% Analysis Date = 02/27/16 Pct Recovery = 92% Analysis Date = 02/22/16 Pct Recovery = 92% Analysis Date = 02/22/16 Pct Recovery = 92% Analysis Date = 02/17/16 Pct Recovery = 92% Analysis Date = 02/17/16 Pct Recovery = 92% Analysis Date = 02/12/16 Pct Recovery = 92% Analysis Date = 02/12/16 Pct Recovery = 92% Analysis Date = 02/07/16 Pct Recovery = 92% Analysis Date = 02/07/16 Pct Recovery = 92% Analysis Date = 02/03/16 Pct Recovery = 92% Analysis Date = 02/03/16 Pct Recovery = 92% Analysis Date = 01/29/16 Pct Recovery = 92% Analysis Date = 01/29/16 Pct Recovery = 92% Analysis Date = 01/24/16 Pct Recovery = 92% Analysis Date = 01/24/16 Pct Recovery = 92% Analysis Date = 01/19/16 Pct Recovery = 92% Analysis Date = 01/19/16 Pct Recovery = 92% Analysis Date = 01/14/16 Pct Recovery = 92% Analysis Date = 01/14/16 Pct Recovery = 92% Analysis Date = 01/10/16 Pct Recovery = 92% Analysis Date = 01/10/16 Pct Recovery = 92% Analysis Date = 01/05/16 Pct Recovery = 92% Analysis Date = 01/05/16 Pct Recovery = 92% Analysis Date = 12/31/15 Pct Recovery = 92% Analysis Date = 12/31/15 Pct Recovery = 92% Analysis Date = 12/26/15 Pct Recovery = 91% Analysis Date = 12/26/15 Pct Recovery = 91% Analysis Date = 12/21/15 Pct Recovery = 91% Analysis Date = 12/21/15 Pct Recovery = 91% Analysis Date = 12/17/15 Pct Recovery = 91% Analysis Date = 12/17/15 Pct Recovery = 91% Analysis Date = 12/12/15 Pct Recovery = 91% Analysis Date = 12/12/15 Pct Recovery = 91% Analysis Date = 12/07/15 Pct Recovery = 91% Analysis Date = 12/07/15 Pct Recovery = 91% Analysis Date = 12/02/15 Pct Recovery = 91% Analysis Date = 12/02/15 Pct Recovery = 91% Analysis Date = 11/27/15 Pct Recovery = 91% Analysis Date = 11/27/15 Pct Recovery = 91% Analysis Date = 11/23/15 Pct Recovery = 91% Analysis Date = 11/23/15 Pct Recovery = 91% Analysis Date = 11/18/15 Pct Recovery = 91% Analysis Date = 11/18/15 Pct Recovery = 91% Analysis Date = 11/13/15 Pct Recovery = 91% Analysis Date = 11/13/15 Pct Recovery = 91% Analysis Date = 11/08/15 Pct Recovery = 91% Analysis Date = 11/08/15 Pct Recovery = 91% Analysis Date = 11/03/15 Pct Recovery = 91% Analysis Date = 11/03/15 Pct Recovery = 91% Analysis Date = 10/30/15 Pct Recovery = 91% Analysis Date = 10/30/15 Pct Recovery = 91% Analysis Date = 10/25/15 Pct Recovery = 91% Analysis Date = 10/25/15 Pct Recovery = 91% Analysis Date = 10/20/15 Pct Recovery = 91% Analysis Date = 10/20/15 Pct Recovery = 91% Analysis Date = 10/15/15 Pct Recovery = 91% Analysis Date = 10/15/15 Pct Recovery = 91% Analysis Date = 10/10/15 Pct Recovery = 91% Analysis Date = 10/10/15 Pct Recovery = 91% Analysis Date = 10/06/15 Pct Recovery = 91% Analysis Date = 10/06/15 Pct Recovery = 91% Analysis Date = 10/01/15 Pct Recovery = 91% Analysis Date = 10/01/15 Pct Recovery = 91% Analysis Date = 09/26/15 Pct Recovery = 91% Analysis Date = 09/26/15 Pct Recovery = 91% Analysis Date = 09/21/15 Pct Recovery = 91% Analysis Date = 09/21/15 Pct Recovery = 91% Analysis Date = 09/16/15 Pct Recovery = 91% Analysis Date = 09/16/15 Pct Recovery = 91% Analysis Date = 09/12/15 Pct Recovery = 91% Analysis Date = 09/12/15 Pct Recovery = 91% Analysis Date = 09/07/15 Pct Recovery = 91% Analysis Date = 09/07/15 Pct Recovery = 91% Analysis Date = 09/02/15 Pct Recovery = 91% Analysis Date = 09/02/15 Pct Recovery = 91% Analysis Date = 08/28/15 Pct Recovery = 91% Analysis Date = 08/28/15 Pct Recovery = 91% Analysis Date = 08/23/15 Pct Recovery = 91% Analysis Date = 08/23/15 Pct Recovery = 91% Analysis Date = 08/19/15 Pct Recovery = 91% Analysis Date = 08/19/15 Pct Recovery = 91% Analysis Date = 08/14/15 Pct Recovery = 91% Analysis Date = 08/14/15 Pct Recovery = 91% Analysis Date = 08/09/15 Pct Recovery = 91% Analysis Date = 08/09/15 Pct Recovery = 91% Analysis Date = 08/04/15 Pct Recovery = 91% Analysis Date = 08/04/15 Pct Recovery = 91% Analysis Date = 07/30/15 Pct Recovery = 91% Analysis Date = 07/30/15 Pct Recovery = 91% Analysis Date = 07/26/15 Pct Recovery = 91% Analysis Date = 07/26/15 Pct Recovery = 91% Analysis Date = 07/21/15 Pct Recovery = 91% Analysis Date = 07/21/15 Pct Recovery = 91% Analysis Date = 07/16/15 Pct Recovery = 91% Analysis Date = 07/16/15 Pct Recovery = 91% Analysis Date = 07/11/15 Pct Recovery = 91% Analysis Date = 07/11/15 Pct Recovery = 91% Analysis Date = 07/06/15 Pct Recovery = 91% Analysis Date = 07/06/15 Pct Recovery = 91% Analysis Date = 07/02/15 Pct Recovery = 91% Analysis Date = 07/02/15 Pct Recovery = 91% Analysis Date = 06/27/15 Pct Recovery = 91% Analysis Date = 06/27/15 Pct Recovery = 91% Analysis Date = 06/22/15 Pct Recovery = 91% Analysis Date = 06/22/15 Pct Recovery = 91% Analysis Date = 06/17/15 Pct Recovery = 91% Analysis Date = 06/17/15 Pct Recovery = 91% Analysis Date = 06/12/15 Pct Recovery = 91% Analysis Date = 06/12/15 Pct Recovery = 91% Analysis Date = 06/08/15 Pct Recovery = 91% Analysis Date = 06/08/15 Pct Recovery = 91% Analysis Date = 06/03/15 Pct Recovery = 91% Analysis Date = 06/03/15 Pct Recovery = 91% Analysis Date = 05/29/15 Pct Recovery = 91% Analysis Date = 05/29/15 Pct Recovery = 91% Analysis Date = 05/24/15 Pct Recovery = 91% Analysis Date = 05/24/15 Pct Recovery = 91% Analysis Date = 05/19/15 Pct Recovery = 91% Analysis Date = 05/19/15 Pct Recovery = 91% Analysis Date = 05/15/15 Pct Recovery = 91% Analysis Date = 05/15/15 Pct Recovery = 91% Analysis Date = 05/10/15 Pct Recovery = 91% Analysis Date = 05/10/15 Pct Recovery = 91% Analysis Date = 05/05/15 Pct Recovery = 91% Analysis Date = 05/05/15 Pct Recovery = 91% Analysis Date = 04/30/15 Pct Recovery = 92% Analysis Date = 04/30/15 Pct Recovery = 92% Analysis Date = 04/25/15 Pct Recovery = 92% Analysis Date = 04/25/15 Pct Recovery = 92% Analysis Date = 04/21/15 Pct Recovery = 92% Analysis Date = 04/21/15 Pct Recovery = 92% Analysis Date = 04/16/15 Pct Recovery = 92% Analysis Date = 04/16/15 Pct Recovery = 92% Analysis Date = 04/11/15 Pct Recovery = 92% Analysis Date = 04/11/15 Pct Recovery = 92% Analysis Date = 04/06/15 Pct Recovery = 92% Analysis Date = 04/06/15 Pct Recovery = 92% Analysis Date = 04/01/15 Pct Recovery = 92% Analysis Date = 04/01/15 Pct Recovery = 92% Analysis Date = 03/28/15 Pct Recovery = 92% Analysis Date = 03/28/15 Pct Recovery = 92% Analysis Date = 03/23/15 Pct Recovery = 92% Analysis Date = 03/23/15 Pct Recovery = 92% Analysis Date = 03/18/15 Pct Recovery = 92% Analysis Date = 03/18/15 Pct Recovery = 92% Analysis Date = 03/13/15 Pct Recovery = 92% Analysis Date = 03/13/15 Pct Recovery = 92% Analysis Date = 03/08/15 Pct Recovery = 93% Analysis Date = 03/08/15 Pct Recovery = 93% Analysis Date = 03/04/15 Pct Recovery = 93% Analysis Date = 03/04/15 Pct Recovery = 93% Analysis Date = 02/27/15 Pct Recovery = 93% Analysis Date = 02/27/15 Pct Recovery = 93% Analysis Date = 02/22/15 Pct Recovery = 93% Analysis Date = 02/22/15 Pct Recovery = 93% Analysis Date = 02/17/15 Pct Recovery = 93% Analysis Date = 02/17/15 Pct Recovery = 93% Analysis Date = 02/12/15 Pct Recovery = 93% Analysis Date = 02/12/15 Pct Recovery = 93% Analysis Date = 02/08/15 Pct Recovery = 93% Analysis Date = 02/08/15 Pct Recovery = 93% Analysis Date = 02/03/15 Pct Recovery = 93% Analysis Date = 02/03/15 Pct Recovery = 93% Analysis Date = 01/29/15 Pct Recovery = 93% Analysis Date = 01/29/15 Pct Recovery = 93% Analysis Date = 01/24/15 Pct Recovery = 93% Analysis Date = 01/24/15 Pct Recovery = 93% Analysis Date = 01/19/15 Pct Recovery = 93% Analysis Date = 01/19/15 Pct Recovery = 93% Analysis Date = 01/15/15 Pct Recovery = 94% Analysis Date = 01/15/15 Pct Recovery = 94% Analysis Date = 01/10/15 Pct Recovery = 94% Analysis Date = 01/10/15 Pct Recovery = 94% Analysis Date = 01/05/15 Pct Recovery = 94% Analysis Date = 01/05/15 Pct Recovery = 94% Analysis Date = 12/31/14 Pct Recovery = 94% Analysis Date = 12/31/14 Pct Recovery = 94% Analysis Date = 12/26/14 Pct Recovery = 94% Analysis Date = 12/26/14 Pct Recovery = 94% Analysis Date = 12/22/14 Pct Recovery = 94% Analysis Date = 12/22/14 Pct Recovery = 94% Analysis Date = 12/17/14 Pct Recovery = 94% Analysis Date = 12/17/14 Pct Recovery = 94% Analysis Date = 12/12/14 Pct Recovery = 94% Analysis Date = 12/12/14 Pct Recovery = 94% Analysis Date = 12/07/14 Pct Recovery = 94% Analysis Date = 12/07/14 Pct Recovery = 94% Analysis Date = 12/02/14 Pct Recovery = 94% Analysis Date = 12/02/14 Pct Recovery = 94% Analysis Date = 11/28/14 Pct Recovery = 94% Analysis Date = 11/28/14 Pct Recovery = 94% Analysis Date = 11/23/14 Pct Recovery = 94% Analysis Date = 11/23/14 Pct Recovery = 94% Analysis Date = 11/18/14 Pct Recovery = 94% Analysis Date = 11/18/14 Pct Recovery = 94% Analysis Date = 11/13/14 Pct Recovery = 94% Analysis Date = 11/13/14 Pct Recovery = 94% Analysis Date = 11/08/14 Pct Recovery = 94% Analysis Date = 11/08/14 Pct Recovery = 94% Analysis Date = 11/04/14 Pct Recovery = 95% Analysis Date = 11/04/14 Pct Recovery = 95% Analysis Date = 10/30/14 Pct Recovery = 95% Analysis Date = 10/30/14 Pct Recovery = 95% Analysis Date = 10/25/14 Pct Recovery = 95% Analysis Date = 10/25/14 Pct Recovery = 95% Analysis Date = 10/20/14 Pct Recovery = 95% Analysis Date = 10/20/14 Pct Recovery = 95% Analysis Date = 10/15/14 Pct Recovery = 95% Analysis Date = 10/15/14 Pct Recovery = 95% Analysis Date = 10/11/14 Pct Recovery = 95% Analysis Date = 10/11/14 Pct Recovery = 95% Analysis Date = 10/06/14 Pct Recovery = 95% Analysis Date = 10/06/14 Pct Recovery = 95% Analysis Date = 10/01/14 Pct Recovery = 95% Analysis Date = 10/01/14 Pct Recovery = 95% Analysis Date = 09/26/14 Pct Recovery = 95% Analysis Date = 09/26/14 Pct Recovery = 95% Analysis Date = 09/21/14 Pct Recovery = 95% Analysis Date = 09/21/14 Pct Recovery = 95% Analysis Date = 09/17/14 Pct Recovery = 95% Analysis Date = 09/17/14 Pct Recovery = 95% Analysis Date = 09/12/14 Pct Recovery = 95% Analysis Date = 09/12/14 Pct Recovery = 95% Analysis Date = 09/07/14 Pct Recovery = 95% Analysis Date = 09/07/14 Pct Recovery = 95% Analysis Date = 09/02/14 Pct Recovery = 95% Analysis Date = 09/02/14 Pct Recovery = 95% Analysis Date = 08/28/14 Pct Recovery = 96% Analysis Date = 08/28/14 Pct Recovery = 96% Analysis Date = 08/24/14 Pct Recovery = 96% Analysis Date = 08/24/14 Pct Recovery = 96% Analysis Date = 08/19/14 Pct Recovery = 96% Analysis Date = 08/19/14 Pct Recovery = 96% Analysis Date = 08/14/14 Pct Recovery = 96% Analysis Date = 08/14/14 Pct Recovery = 96% Analysis Date = 08/09/14 Pct Recovery = 96% Analysis Date = 08/09/14 Pct Recovery = 96% Analysis Date = 08/04/14 Pct Recovery = 96% Analysis Date = 08/04/14 Pct Recovery = 96% Analysis Date = 07/31/14 Pct Recovery = 96% Analysis Date = 07/31/14 Pct Recovery = 96% Analysis Date = 07/26/14 Pct Recovery = 96% Analysis Date = 07/26/14 Pct Recovery = 96% Analysis Date = 07/21/14 Pct Recovery = 96% Analysis Date = 07/21/14 Pct Recovery = 96% Analysis Date = 07/16/14 Pct Recovery = 96% Analysis Date = 07/16/14 Pct Recovery = 96% Analysis Date = 07/11/14 Pct Recovery = 96% Analysis Date = 07/11/14 Pct Recovery = 96% Analysis Date = 07/07/14 Pct Recovery = 96% Analysis Date = 07/07/14 Pct Recovery = 96% Analysis Date = 07/02/14 Pct Recovery = 96% Analysis Date = 07/02/14 Pct Recovery = 96% Analysis Date = 06/27/14 Pct Recovery = 96% Analysis Date = 06/27/14 Pct Recovery = 96% Analysis Date = 06/22/14 Pct Recovery = 96% Analysis Date = 06/22/14 Pct Recovery = 96% Analysis Date = 06/17/14 Pct Recovery = 97% Analysis Date = 06/17/14 Pct Recovery = 97% Analysis Date = 06/13/14 Pct Recovery = 97% Analysis Date = 06/13/14 Pct Recovery = 97% Analysis Date = 06/08/14 Pct Recovery = 97% Analysis Date = 06/08/14 Pct Recovery = 97% Analysis Date = 06/03/14 Pct Recovery = 97% Analysis Date = 06/03/14 Pct Recovery = 97% Analysis Date = 05/29/14 Pct Recovery = 97% Analysis Date = 05/29/14 Pct Recovery = 97% Analysis Date = 05/24/14 Pct Recovery = 97% Analysis Date = 05/24/14 Pct Recovery = 97% Analysis Date = 05/20/14 Pct Recovery = 97% Analysis Date = 05/20/14 Pct Recovery = 97% Analysis Date = 05/15/14 Pct Recovery = 97% Analysis Date = 05/15/14 Pct Recovery = 97% Analysis Date = 05/10/14 Pct Recovery = 97% Analysis Date = 05/10/14 Pct Recovery = 97% Analysis Date = 05/05/14 Pct Recovery = 97% Analysis Date = 05/05/14 Pct Recovery = 97% Analysis Date = 05/01/14 Pct Recovery = 97% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
1,1,1,2-TETRACHLOROETHANE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 48 94% 6% 92% 7%
Total 48 94% 6% 92% 7%

Sample Statistics
1,1,1,2-TETRACHLOROETHANE

Characteristic N % % Basis
Plotted 48 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 48 .  
False Negatives 0 0% 0 out of 48
Not Spiked 25 .  
False Positives 0 0% 0 out of 25

BQS OBSP Determination:
1,1,1-TRICHLOROETHANE
METHOD: 4440 , TESTIDCODE: 34506GCM66
Open Data Set

Analysis Date = 12/12/16 SpikeMix = Accu 216041125: 40 µl & Crescent 03FF058: 40 µl Pct Recovery = 92% Analysis Date = 08/04/16 SpikeMix = Crescent 03FF058: 40 µl & Supelco LC20141V: 40 µl Pct Recovery = 88% Analysis Date = 11/21/16 SpikeMix = Crescent 03FF058: 25 µl & Supelco LC20141V: 25 µl Pct Recovery = 88% Analysis Date = 06/30/16 SpikeMix = Crescent 03FF058: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 94% Analysis Date = 06/21/16 SpikeMix = Phenova B20160319: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 86% Analysis Date = 05/24/16 SpikeMix = Accu 216041125: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 86% Analysis Date = 04/09/15 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 105% Analysis Date = 03/19/15 SpikeMix = Spex Organics C1140417015: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 95% Analysis Date = 12/17/14 SpikeMix = Supelco LC06438: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 84% Analysis Date = 11/14/14 SpikeMix = Crescent 03DD004: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 82% Analysis Date = 08/19/14 SpikeMix = Spex Organics C1140417015: 20 µl & Accu 214031115: 20 µl Pct Recovery = 98% Analysis Date = 07/01/14 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 108% Analysis Date = 06/10/14 SpikeMix = Crescent 03DD004: 20 µl & NSI 032614: 20 µl Pct Recovery = 92% Analysis Date = 05/01/14 SpikeMix = Accu 214031115: 20 µl & NSI 032614: 20 µl Pct Recovery = 102% Analysis Date = 08/15/15 SpikeMix = Supelco LC13545: 25 µl & Crescent 04EE008: 25 µl Pct Recovery = 97% Analysis Date = 06/16/15 SpikeMix = ERA 0406-15-03: 25 µl & Supelco LC13545: 25 µl Pct Recovery = 88% Analysis Date = 09/28/16 SpikeMix = Crescent 03FF058: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 95% Analysis Date = 09/08/16 SpikeMix = Phenova B20160319: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 83% Analysis Date = 08/20/16 SpikeMix = Accu 216041125: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 89% Analysis Date = 04/26/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 94% Analysis Date = 02/05/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 93% Analysis Date = 11/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 93% Analysis Date = 10/16/15 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 96% Analysis Date = 05/09/15 SpikeMix = Spex Organics EN150428007: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 99% Analysis Date = 04/02/16 SpikeMix = Supelco LC13545: 15 µl & Accu 215041380: 15 µl Pct Recovery = 97% Analysis Date = 12/18/15 SpikeMix = Supelco LC13545: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 79% Analysis Date = 01/13/15 SpikeMix = Accu 214031115: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 98% Analysis Date = 11/06/14 SpikeMix = Spex Organics C1140417015: 10 µl & Crescent 03DD004: 10 µl Pct Recovery = 88% Analysis Date = 10/04/14 SpikeMix = Crescent 03DD004: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 99% Analysis Date = 09/09/14 SpikeMix = Accu 214031115: 10 µl & NSI 032614: 10 µl Pct Recovery = 115% Analysis Date = 07/29/14 SpikeMix = Crescent 03DD004: 10 µl & NSI 032614: 10 µl Pct Recovery = 104% Analysis Date = 07/23/14 SpikeMix = Spex Organics C1140417015: 10 µl & Accu 214031115: 10 µl Pct Recovery = 117% Analysis Date = 06/18/14 SpikeMix = Supelco LC06438: 10 µl & Accu 214031115: 10 µl Pct Recovery = 119% Analysis Date = 05/03/14 SpikeMix = Crescent 03DD004: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 96% Analysis Date = 02/18/16 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 107% Analysis Date = 11/12/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 100% Analysis Date = 09/03/15 SpikeMix = NSI 050515AVOC: 10 µl & Spex Organics EN150428007: 10 µl Pct Recovery = 100% Analysis Date = 05/21/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 105% Analysis Date = 05/13/16 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 117% Analysis Date = 03/17/16 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 103% Analysis Date = 12/10/15 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 96% Analysis Date = 06/27/15 SpikeMix = ERA 0406-15-03: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 97% Analysis Date = 05/09/15 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 97% Analysis Date = 12/11/16 Pct Recovery = 89% Analysis Date = 12/07/16 Pct Recovery = 89% Analysis Date = 12/07/16 Pct Recovery = 89% Analysis Date = 12/02/16 Pct Recovery = 89% Analysis Date = 12/02/16 Pct Recovery = 89% Analysis Date = 11/27/16 Pct Recovery = 89% Analysis Date = 11/27/16 Pct Recovery = 89% Analysis Date = 11/22/16 Pct Recovery = 90% Analysis Date = 11/22/16 Pct Recovery = 90% Analysis Date = 11/18/16 Pct Recovery = 90% Analysis Date = 11/18/16 Pct Recovery = 90% Analysis Date = 11/13/16 Pct Recovery = 90% Analysis Date = 11/13/16 Pct Recovery = 90% Analysis Date = 11/08/16 Pct Recovery = 90% Analysis Date = 11/08/16 Pct Recovery = 90% Analysis Date = 11/03/16 Pct Recovery = 90% Analysis Date = 11/03/16 Pct Recovery = 90% Analysis Date = 10/29/16 Pct Recovery = 90% Analysis Date = 10/29/16 Pct Recovery = 90% Analysis Date = 10/25/16 Pct Recovery = 90% Analysis Date = 10/25/16 Pct Recovery = 90% Analysis Date = 10/20/16 Pct Recovery = 90% Analysis Date = 10/20/16 Pct Recovery = 90% Analysis Date = 10/15/16 Pct Recovery = 90% Analysis Date = 10/15/16 Pct Recovery = 90% Analysis Date = 10/10/16 Pct Recovery = 91% Analysis Date = 10/10/16 Pct Recovery = 91% Analysis Date = 10/06/16 Pct Recovery = 91% Analysis Date = 10/06/16 Pct Recovery = 91% Analysis Date = 10/01/16 Pct Recovery = 91% Analysis Date = 10/01/16 Pct Recovery = 91% Analysis Date = 09/26/16 Pct Recovery = 91% Analysis Date = 09/26/16 Pct Recovery = 91% Analysis Date = 09/21/16 Pct Recovery = 91% Analysis Date = 09/21/16 Pct Recovery = 91% Analysis Date = 09/16/16 Pct Recovery = 91% Analysis Date = 09/16/16 Pct Recovery = 91% Analysis Date = 09/12/16 Pct Recovery = 91% Analysis Date = 09/12/16 Pct Recovery = 91% Analysis Date = 09/07/16 Pct Recovery = 91% Analysis Date = 09/07/16 Pct Recovery = 91% Analysis Date = 09/02/16 Pct Recovery = 92% Analysis Date = 09/02/16 Pct Recovery = 92% Analysis Date = 08/28/16 Pct Recovery = 92% Analysis Date = 08/28/16 Pct Recovery = 92% Analysis Date = 08/24/16 Pct Recovery = 92% Analysis Date = 08/24/16 Pct Recovery = 92% Analysis Date = 08/19/16 Pct Recovery = 92% Analysis Date = 08/19/16 Pct Recovery = 92% Analysis Date = 08/14/16 Pct Recovery = 92% Analysis Date = 08/14/16 Pct Recovery = 92% Analysis Date = 08/09/16 Pct Recovery = 92% Analysis Date = 08/09/16 Pct Recovery = 92% Analysis Date = 08/04/16 Pct Recovery = 92% Analysis Date = 08/04/16 Pct Recovery = 92% Analysis Date = 07/31/16 Pct Recovery = 92% Analysis Date = 07/31/16 Pct Recovery = 92% Analysis Date = 07/26/16 Pct Recovery = 92% Analysis Date = 07/26/16 Pct Recovery = 92% Analysis Date = 07/21/16 Pct Recovery = 93% Analysis Date = 07/21/16 Pct Recovery = 93% Analysis Date = 07/16/16 Pct Recovery = 93% Analysis Date = 07/16/16 Pct Recovery = 93% Analysis Date = 07/12/16 Pct Recovery = 93% Analysis Date = 07/12/16 Pct Recovery = 93% Analysis Date = 07/07/16 Pct Recovery = 93% Analysis Date = 07/07/16 Pct Recovery = 93% Analysis Date = 07/02/16 Pct Recovery = 93% Analysis Date = 07/02/16 Pct Recovery = 93% Analysis Date = 06/27/16 Pct Recovery = 93% Analysis Date = 06/27/16 Pct Recovery = 93% Analysis Date = 06/22/16 Pct Recovery = 93% Analysis Date = 06/22/16 Pct Recovery = 93% Analysis Date = 06/18/16 Pct Recovery = 93% Analysis Date = 06/18/16 Pct Recovery = 93% Analysis Date = 06/13/16 Pct Recovery = 93% Analysis Date = 06/13/16 Pct Recovery = 93% Analysis Date = 06/08/16 Pct Recovery = 93% Analysis Date = 06/08/16 Pct Recovery = 93% Analysis Date = 06/03/16 Pct Recovery = 93% Analysis Date = 06/03/16 Pct Recovery = 93% Analysis Date = 05/30/16 Pct Recovery = 94% Analysis Date = 05/30/16 Pct Recovery = 94% Analysis Date = 05/25/16 Pct Recovery = 94% Analysis Date = 05/25/16 Pct Recovery = 94% Analysis Date = 05/20/16 Pct Recovery = 94% Analysis Date = 05/20/16 Pct Recovery = 94% Analysis Date = 05/15/16 Pct Recovery = 94% Analysis Date = 05/15/16 Pct Recovery = 94% Analysis Date = 05/10/16 Pct Recovery = 94% Analysis Date = 05/10/16 Pct Recovery = 94% Analysis Date = 05/06/16 Pct Recovery = 94% Analysis Date = 05/06/16 Pct Recovery = 94% Analysis Date = 05/01/16 Pct Recovery = 94% Analysis Date = 05/01/16 Pct Recovery = 94% Analysis Date = 04/26/16 Pct Recovery = 94% Analysis Date = 04/26/16 Pct Recovery = 94% Analysis Date = 04/21/16 Pct Recovery = 94% Analysis Date = 04/21/16 Pct Recovery = 94% Analysis Date = 04/16/16 Pct Recovery = 94% Analysis Date = 04/16/16 Pct Recovery = 94% Analysis Date = 04/12/16 Pct Recovery = 94% Analysis Date = 04/12/16 Pct Recovery = 94% Analysis Date = 04/07/16 Pct Recovery = 95% Analysis Date = 04/07/16 Pct Recovery = 95% Analysis Date = 04/02/16 Pct Recovery = 95% Analysis Date = 04/02/16 Pct Recovery = 95% Analysis Date = 03/28/16 Pct Recovery = 95% Analysis Date = 03/28/16 Pct Recovery = 95% Analysis Date = 03/24/16 Pct Recovery = 95% Analysis Date = 03/24/16 Pct Recovery = 95% Analysis Date = 03/19/16 Pct Recovery = 95% Analysis Date = 03/19/16 Pct Recovery = 95% Analysis Date = 03/14/16 Pct Recovery = 95% Analysis Date = 03/14/16 Pct Recovery = 95% Analysis Date = 03/09/16 Pct Recovery = 95% Analysis Date = 03/09/16 Pct Recovery = 95% Analysis Date = 03/04/16 Pct Recovery = 95% Analysis Date = 03/04/16 Pct Recovery = 95% Analysis Date = 02/29/16 Pct Recovery = 95% Analysis Date = 02/29/16 Pct Recovery = 95% Analysis Date = 02/24/16 Pct Recovery = 95% Analysis Date = 02/24/16 Pct Recovery = 95% Analysis Date = 02/19/16 Pct Recovery = 95% Analysis Date = 02/19/16 Pct Recovery = 95% Analysis Date = 02/14/16 Pct Recovery = 95% Analysis Date = 02/14/16 Pct Recovery = 95% Analysis Date = 02/10/16 Pct Recovery = 95% Analysis Date = 02/10/16 Pct Recovery = 95% Analysis Date = 02/05/16 Pct Recovery = 96% Analysis Date = 02/05/16 Pct Recovery = 96% Analysis Date = 01/31/16 Pct Recovery = 96% Analysis Date = 01/31/16 Pct Recovery = 96% Analysis Date = 01/26/16 Pct Recovery = 96% Analysis Date = 01/26/16 Pct Recovery = 96% Analysis Date = 01/21/16 Pct Recovery = 96% Analysis Date = 01/21/16 Pct Recovery = 96% Analysis Date = 01/17/16 Pct Recovery = 96% Analysis Date = 01/17/16 Pct Recovery = 96% Analysis Date = 01/12/16 Pct Recovery = 96% Analysis Date = 01/12/16 Pct Recovery = 96% Analysis Date = 01/07/16 Pct Recovery = 96% Analysis Date = 01/07/16 Pct Recovery = 96% Analysis Date = 01/02/16 Pct Recovery = 96% Analysis Date = 01/02/16 Pct Recovery = 96% Analysis Date = 12/29/15 Pct Recovery = 96% Analysis Date = 12/29/15 Pct Recovery = 96% Analysis Date = 12/24/15 Pct Recovery = 96% Analysis Date = 12/24/15 Pct Recovery = 96% Analysis Date = 12/19/15 Pct Recovery = 96% Analysis Date = 12/19/15 Pct Recovery = 96% Analysis Date = 12/14/15 Pct Recovery = 96% Analysis Date = 12/14/15 Pct Recovery = 96% Analysis Date = 12/09/15 Pct Recovery = 96% Analysis Date = 12/09/15 Pct Recovery = 96% Analysis Date = 12/05/15 Pct Recovery = 96% Analysis Date = 12/05/15 Pct Recovery = 96% Analysis Date = 11/30/15 Pct Recovery = 96% Analysis Date = 11/30/15 Pct Recovery = 96% Analysis Date = 11/25/15 Pct Recovery = 96% Analysis Date = 11/25/15 Pct Recovery = 96% Analysis Date = 11/20/15 Pct Recovery = 97% Analysis Date = 11/20/15 Pct Recovery = 97% Analysis Date = 11/16/15 Pct Recovery = 97% Analysis Date = 11/16/15 Pct Recovery = 97% Analysis Date = 11/11/15 Pct Recovery = 97% Analysis Date = 11/11/15 Pct Recovery = 97% Analysis Date = 11/06/15 Pct Recovery = 97% Analysis Date = 11/06/15 Pct Recovery = 97% Analysis Date = 11/01/15 Pct Recovery = 97% Analysis Date = 11/01/15 Pct Recovery = 97% Analysis Date = 10/27/15 Pct Recovery = 97% Analysis Date = 10/27/15 Pct Recovery = 97% Analysis Date = 10/23/15 Pct Recovery = 97% Analysis Date = 10/23/15 Pct Recovery = 97% Analysis Date = 10/18/15 Pct Recovery = 97% Analysis Date = 10/18/15 Pct Recovery = 97% Analysis Date = 10/13/15 Pct Recovery = 97% Analysis Date = 10/13/15 Pct Recovery = 97% Analysis Date = 10/08/15 Pct Recovery = 97% Analysis Date = 10/08/15 Pct Recovery = 97% Analysis Date = 10/04/15 Pct Recovery = 97% Analysis Date = 10/04/15 Pct Recovery = 97% Analysis Date = 09/29/15 Pct Recovery = 97% Analysis Date = 09/29/15 Pct Recovery = 97% Analysis Date = 09/24/15 Pct Recovery = 97% Analysis Date = 09/24/15 Pct Recovery = 97% Analysis Date = 09/19/15 Pct Recovery = 97% Analysis Date = 09/19/15 Pct Recovery = 97% Analysis Date = 09/14/15 Pct Recovery = 97% Analysis Date = 09/14/15 Pct Recovery = 97% Analysis Date = 09/10/15 Pct Recovery = 97% Analysis Date = 09/10/15 Pct Recovery = 97% Analysis Date = 09/05/15 Pct Recovery = 97% Analysis Date = 09/05/15 Pct Recovery = 97% Analysis Date = 08/31/15 Pct Recovery = 97% Analysis Date = 08/31/15 Pct Recovery = 97% Analysis Date = 08/26/15 Pct Recovery = 97% Analysis Date = 08/26/15 Pct Recovery = 97% Analysis Date = 08/21/15 Pct Recovery = 97% Analysis Date = 08/21/15 Pct Recovery = 97% Analysis Date = 08/17/15 Pct Recovery = 97% Analysis Date = 08/17/15 Pct Recovery = 97% Analysis Date = 08/12/15 Pct Recovery = 97% Analysis Date = 08/12/15 Pct Recovery = 97% Analysis Date = 08/07/15 Pct Recovery = 97% Analysis Date = 08/07/15 Pct Recovery = 97% Analysis Date = 08/02/15 Pct Recovery = 97% Analysis Date = 08/02/15 Pct Recovery = 97% Analysis Date = 07/29/15 Pct Recovery = 97% Analysis Date = 07/29/15 Pct Recovery = 97% Analysis Date = 07/24/15 Pct Recovery = 96% Analysis Date = 07/24/15 Pct Recovery = 96% Analysis Date = 07/19/15 Pct Recovery = 96% Analysis Date = 07/19/15 Pct Recovery = 96% Analysis Date = 07/14/15 Pct Recovery = 96% Analysis Date = 07/14/15 Pct Recovery = 96% Analysis Date = 07/09/15 Pct Recovery = 96% Analysis Date = 07/09/15 Pct Recovery = 96% Analysis Date = 07/05/15 Pct Recovery = 96% Analysis Date = 07/05/15 Pct Recovery = 96% Analysis Date = 06/30/15 Pct Recovery = 96% Analysis Date = 06/30/15 Pct Recovery = 96% Analysis Date = 06/25/15 Pct Recovery = 96% Analysis Date = 06/25/15 Pct Recovery = 96% Analysis Date = 06/20/15 Pct Recovery = 96% Analysis Date = 06/20/15 Pct Recovery = 96% Analysis Date = 06/16/15 Pct Recovery = 96% Analysis Date = 06/16/15 Pct Recovery = 96% Analysis Date = 06/11/15 Pct Recovery = 96% Analysis Date = 06/11/15 Pct Recovery = 96% Analysis Date = 06/06/15 Pct Recovery = 96% Analysis Date = 06/06/15 Pct Recovery = 96% Analysis Date = 06/01/15 Pct Recovery = 96% Analysis Date = 06/01/15 Pct Recovery = 96% Analysis Date = 05/27/15 Pct Recovery = 96% Analysis Date = 05/27/15 Pct Recovery = 96% Analysis Date = 05/23/15 Pct Recovery = 96% Analysis Date = 05/23/15 Pct Recovery = 96% Analysis Date = 05/18/15 Pct Recovery = 96% Analysis Date = 05/18/15 Pct Recovery = 96% Analysis Date = 05/13/15 Pct Recovery = 96% Analysis Date = 05/13/15 Pct Recovery = 96% Analysis Date = 05/08/15 Pct Recovery = 96% Analysis Date = 05/08/15 Pct Recovery = 96% Analysis Date = 05/04/15 Pct Recovery = 96% Analysis Date = 05/04/15 Pct Recovery = 96% Analysis Date = 04/29/15 Pct Recovery = 96% Analysis Date = 04/29/15 Pct Recovery = 96% Analysis Date = 04/24/15 Pct Recovery = 96% Analysis Date = 04/24/15 Pct Recovery = 96% Analysis Date = 04/19/15 Pct Recovery = 96% Analysis Date = 04/19/15 Pct Recovery = 96% Analysis Date = 04/14/15 Pct Recovery = 96% Analysis Date = 04/14/15 Pct Recovery = 96% Analysis Date = 04/10/15 Pct Recovery = 96% Analysis Date = 04/10/15 Pct Recovery = 96% Analysis Date = 04/05/15 Pct Recovery = 97% Analysis Date = 04/05/15 Pct Recovery = 97% Analysis Date = 03/31/15 Pct Recovery = 97% Analysis Date = 03/31/15 Pct Recovery = 97% Analysis Date = 03/26/15 Pct Recovery = 97% Analysis Date = 03/26/15 Pct Recovery = 97% Analysis Date = 03/22/15 Pct Recovery = 97% Analysis Date = 03/22/15 Pct Recovery = 97% Analysis Date = 03/17/15 Pct Recovery = 97% Analysis Date = 03/17/15 Pct Recovery = 97% Analysis Date = 03/12/15 Pct Recovery = 97% Analysis Date = 03/12/15 Pct Recovery = 97% Analysis Date = 03/07/15 Pct Recovery = 97% Analysis Date = 03/07/15 Pct Recovery = 97% Analysis Date = 03/02/15 Pct Recovery = 97% Analysis Date = 03/02/15 Pct Recovery = 97% Analysis Date = 02/26/15 Pct Recovery = 97% Analysis Date = 02/26/15 Pct Recovery = 97% Analysis Date = 02/21/15 Pct Recovery = 97% Analysis Date = 02/21/15 Pct Recovery = 97% Analysis Date = 02/16/15 Pct Recovery = 97% Analysis Date = 02/16/15 Pct Recovery = 97% Analysis Date = 02/11/15 Pct Recovery = 97% Analysis Date = 02/11/15 Pct Recovery = 97% Analysis Date = 02/07/15 Pct Recovery = 97% Analysis Date = 02/07/15 Pct Recovery = 97% Analysis Date = 02/02/15 Pct Recovery = 97% Analysis Date = 02/02/15 Pct Recovery = 97% Analysis Date = 01/28/15 Pct Recovery = 98% Analysis Date = 01/28/15 Pct Recovery = 98% Analysis Date = 01/23/15 Pct Recovery = 98% Analysis Date = 01/23/15 Pct Recovery = 98% Analysis Date = 01/18/15 Pct Recovery = 98% Analysis Date = 01/18/15 Pct Recovery = 98% Analysis Date = 01/14/15 Pct Recovery = 98% Analysis Date = 01/14/15 Pct Recovery = 98% Analysis Date = 01/09/15 Pct Recovery = 98% Analysis Date = 01/09/15 Pct Recovery = 98% Analysis Date = 01/04/15 Pct Recovery = 98% Analysis Date = 01/04/15 Pct Recovery = 98% Analysis Date = 12/30/14 Pct Recovery = 98% Analysis Date = 12/30/14 Pct Recovery = 98% Analysis Date = 12/25/14 Pct Recovery = 98% Analysis Date = 12/25/14 Pct Recovery = 98% Analysis Date = 12/21/14 Pct Recovery = 98% Analysis Date = 12/21/14 Pct Recovery = 98% Analysis Date = 12/16/14 Pct Recovery = 99% Analysis Date = 12/16/14 Pct Recovery = 99% Analysis Date = 12/11/14 Pct Recovery = 99% Analysis Date = 12/11/14 Pct Recovery = 99% Analysis Date = 12/06/14 Pct Recovery = 99% Analysis Date = 12/06/14 Pct Recovery = 99% Analysis Date = 12/02/14 Pct Recovery = 99% Analysis Date = 12/02/14 Pct Recovery = 99% Analysis Date = 11/27/14 Pct Recovery = 99% Analysis Date = 11/27/14 Pct Recovery = 99% Analysis Date = 11/22/14 Pct Recovery = 99% Analysis Date = 11/22/14 Pct Recovery = 99% Analysis Date = 11/17/14 Pct Recovery = 99% Analysis Date = 11/17/14 Pct Recovery = 99% Analysis Date = 11/12/14 Pct Recovery = 99% Analysis Date = 11/12/14 Pct Recovery = 99% Analysis Date = 11/08/14 Pct Recovery = 100% Analysis Date = 11/08/14 Pct Recovery = 100% Analysis Date = 11/03/14 Pct Recovery = 100% Analysis Date = 11/03/14 Pct Recovery = 100% Analysis Date = 10/29/14 Pct Recovery = 100% Analysis Date = 10/29/14 Pct Recovery = 100% Analysis Date = 10/24/14 Pct Recovery = 100% Analysis Date = 10/24/14 Pct Recovery = 100% Analysis Date = 10/20/14 Pct Recovery = 100% Analysis Date = 10/20/14 Pct Recovery = 100% Analysis Date = 10/15/14 Pct Recovery = 100% Analysis Date = 10/15/14 Pct Recovery = 100% Analysis Date = 10/10/14 Pct Recovery = 100% Analysis Date = 10/10/14 Pct Recovery = 100% Analysis Date = 10/05/14 Pct Recovery = 100% Analysis Date = 10/05/14 Pct Recovery = 100% Analysis Date = 09/30/14 Pct Recovery = 100% Analysis Date = 09/30/14 Pct Recovery = 100% Analysis Date = 09/26/14 Pct Recovery = 101% Analysis Date = 09/26/14 Pct Recovery = 101% Analysis Date = 09/21/14 Pct Recovery = 101% Analysis Date = 09/21/14 Pct Recovery = 101% Analysis Date = 09/16/14 Pct Recovery = 101% Analysis Date = 09/16/14 Pct Recovery = 101% Analysis Date = 09/11/14 Pct Recovery = 101% Analysis Date = 09/11/14 Pct Recovery = 101% Analysis Date = 09/07/14 Pct Recovery = 101% Analysis Date = 09/07/14 Pct Recovery = 101% Analysis Date = 09/02/14 Pct Recovery = 101% Analysis Date = 09/02/14 Pct Recovery = 101% Analysis Date = 08/28/14 Pct Recovery = 101% Analysis Date = 08/28/14 Pct Recovery = 101% Analysis Date = 08/23/14 Pct Recovery = 101% Analysis Date = 08/23/14 Pct Recovery = 101% Analysis Date = 08/18/14 Pct Recovery = 101% Analysis Date = 08/18/14 Pct Recovery = 101% Analysis Date = 08/14/14 Pct Recovery = 102% Analysis Date = 08/14/14 Pct Recovery = 102% Analysis Date = 08/09/14 Pct Recovery = 102% Analysis Date = 08/09/14 Pct Recovery = 102% Analysis Date = 08/04/14 Pct Recovery = 102% Analysis Date = 08/04/14 Pct Recovery = 102% Analysis Date = 07/30/14 Pct Recovery = 102% Analysis Date = 07/30/14 Pct Recovery = 102% Analysis Date = 07/26/14 Pct Recovery = 102% Analysis Date = 07/26/14 Pct Recovery = 102% Analysis Date = 07/21/14 Pct Recovery = 102% Analysis Date = 07/21/14 Pct Recovery = 102% Analysis Date = 07/16/14 Pct Recovery = 102% Analysis Date = 07/16/14 Pct Recovery = 102% Analysis Date = 07/11/14 Pct Recovery = 102% Analysis Date = 07/11/14 Pct Recovery = 102% Analysis Date = 07/06/14 Pct Recovery = 103% Analysis Date = 07/06/14 Pct Recovery = 103% Analysis Date = 07/02/14 Pct Recovery = 103% Analysis Date = 07/02/14 Pct Recovery = 103% Analysis Date = 06/27/14 Pct Recovery = 103% Analysis Date = 06/27/14 Pct Recovery = 103% Analysis Date = 06/22/14 Pct Recovery = 103% Analysis Date = 06/22/14 Pct Recovery = 103% Analysis Date = 06/17/14 Pct Recovery = 103% Analysis Date = 06/17/14 Pct Recovery = 103% Analysis Date = 06/13/14 Pct Recovery = 103% Analysis Date = 06/13/14 Pct Recovery = 103% Analysis Date = 06/08/14 Pct Recovery = 103% Analysis Date = 06/08/14 Pct Recovery = 103% Analysis Date = 06/03/14 Pct Recovery = 104% Analysis Date = 06/03/14 Pct Recovery = 104% Analysis Date = 05/29/14 Pct Recovery = 104% Analysis Date = 05/29/14 Pct Recovery = 104% Analysis Date = 05/24/14 Pct Recovery = 104% Analysis Date = 05/24/14 Pct Recovery = 104% Analysis Date = 05/20/14 Pct Recovery = 104% Analysis Date = 05/20/14 Pct Recovery = 104% Analysis Date = 05/15/14 Pct Recovery = 104% Analysis Date = 05/15/14 Pct Recovery = 104% Analysis Date = 05/10/14 Pct Recovery = 104% Analysis Date = 05/10/14 Pct Recovery = 104% Analysis Date = 05/05/14 Pct Recovery = 104% Analysis Date = 05/05/14 Pct Recovery = 104% Analysis Date = 05/01/14 Pct Recovery = 105% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
1,1,1-TRICHLOROETHANE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 43 97% 9% 96% 9%
Total 43 97% 9% 96% 9%

Sample Statistics
1,1,1-TRICHLOROETHANE

Characteristic N % % Basis
Plotted 43 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 43 .  
False Negatives 0 0% 0 out of 43
Not Spiked 23 .  
False Positives 0 0% 0 out of 23

BQS OBSP Determination:
1,1,2,2-TETRACHLOROETHANE
METHOD: 4440 , TESTIDCODE: 34516GCM66
Open Data Set

Analysis Date = 12/16/16 SpikeMix = NSI 041816AVOC: 40 µl & ChemService 5082900: 40 µl Pct Recovery = 95% Analysis Date = 08/04/16 SpikeMix = Crescent 03FF058: 40 µl & Supelco LC20141V: 40 µl Pct Recovery = 91% Analysis Date = 07/20/16 SpikeMix = Supelco LC20141V: 40 µl & Accu 216041125: 40 µl Pct Recovery = 87% Analysis Date = 08/26/16 SpikeMix = NSI 041816AVOC: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 101% Analysis Date = 08/12/16 SpikeMix = ChemService 5082900: 25 µl & Phenova B20160319: 25 µl Pct Recovery = 91% Analysis Date = 06/30/16 SpikeMix = Crescent 03FF058: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 96% Analysis Date = 11/21/16 SpikeMix = Crescent 03FF058: 25 µl & Supelco LC20141V: 25 µl Pct Recovery = 92% Analysis Date = 09/08/16 SpikeMix = Supelco LC20141V: 25 µl & Accu 216041125: 25 µl Pct Recovery = 94% Analysis Date = 11/22/14 SpikeMix = NSI 032614: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 81% Analysis Date = 06/10/14 SpikeMix = Crescent 03DD004: 20 µl & NSI 032614: 20 µl Pct Recovery = 89% Analysis Date = 06/10/14 SpikeMix = NSI 032614: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 91% Analysis Date = 05/01/14 SpikeMix = Accu 214031115: 20 µl & NSI 032614: 20 µl Pct Recovery = 87% Analysis Date = 04/09/15 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 93% Analysis Date = 03/06/15 SpikeMix = ERA 0227-14-06.1A: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 96% Analysis Date = 11/14/14 SpikeMix = Crescent 03DD004: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 90% Analysis Date = 08/16/14 SpikeMix = ERA 0227-14-06.1A: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 92% Analysis Date = 07/01/14 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 102% Analysis Date = 08/15/15 SpikeMix = Supelco LC13545: 25 µl & Crescent 04EE008: 25 µl Pct Recovery = 99% Analysis Date = 06/16/15 SpikeMix = ERA 0406-15-03: 25 µl & Supelco LC13545: 25 µl Pct Recovery = 88% Analysis Date = 11/29/16 SpikeMix = ChemService 5082900: 15 µl & Phenova B20160319: 15 µl Pct Recovery = 93% Analysis Date = 09/28/16 SpikeMix = Crescent 03FF058: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 97% Analysis Date = 06/30/16 SpikeMix = ChemService 5082900: 15 µl & Accu 216041125: 15 µl Pct Recovery = 96% Analysis Date = 06/10/16 SpikeMix = NSI 041816AVOC: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 87% Analysis Date = 10/13/16 SpikeMix = NSI 041816AVOC: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 92% Analysis Date = 05/27/16 SpikeMix = Phenova B20160319: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 93% Analysis Date = 04/26/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 108% Analysis Date = 02/05/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 79% Analysis Date = 11/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 93% Analysis Date = 10/16/15 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 92% Analysis Date = 05/09/15 SpikeMix = Spex Organics EN150428007: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 95% Analysis Date = 04/02/16 SpikeMix = Supelco LC13545: 15 µl & Accu 215041380: 15 µl Pct Recovery = 88% Analysis Date = 12/18/15 SpikeMix = Supelco LC13545: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 87% Analysis Date = 09/09/14 SpikeMix = Accu 214031115: 10 µl & NSI 032614: 10 µl Pct Recovery = 90% Analysis Date = 09/09/14 SpikeMix = NSI 032614: 10 µl & Spex Organics C1140417015: 10 µl Pct Recovery = 99% Analysis Date = 07/29/14 SpikeMix = Crescent 03DD004: 10 µl & NSI 032614: 10 µl Pct Recovery = 99% Analysis Date = 05/30/14 SpikeMix = NSI 032614: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 80% Analysis Date = 01/13/15 SpikeMix = Accu 214031115: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 79% Analysis Date = 10/21/14 SpikeMix = ERA 0227-14-06.1A: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 87% Analysis Date = 10/04/14 SpikeMix = Crescent 03DD004: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 95% Analysis Date = 07/11/14 SpikeMix = Spex Organics C1140417015: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 95% Analysis Date = 02/18/16 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 94% Analysis Date = 11/12/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 87% Analysis Date = 09/03/15 SpikeMix = NSI 050515AVOC: 10 µl & Spex Organics EN150428007: 10 µl Pct Recovery = 94% Analysis Date = 05/21/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 96% Analysis Date = 05/13/16 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 97% Analysis Date = 03/17/16 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 84% Analysis Date = 12/10/15 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 99% Analysis Date = 06/27/15 SpikeMix = ERA 0406-15-03: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 90% Analysis Date = 05/09/15 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 87% Analysis Date = 12/15/16 Pct Recovery = 95% Analysis Date = 12/11/16 Pct Recovery = 95% Analysis Date = 12/11/16 Pct Recovery = 95% Analysis Date = 12/06/16 Pct Recovery = 94% Analysis Date = 12/06/16 Pct Recovery = 94% Analysis Date = 12/01/16 Pct Recovery = 94% Analysis Date = 12/01/16 Pct Recovery = 94% Analysis Date = 11/26/16 Pct Recovery = 94% Analysis Date = 11/26/16 Pct Recovery = 94% Analysis Date = 11/21/16 Pct Recovery = 94% Analysis Date = 11/21/16 Pct Recovery = 94% Analysis Date = 11/17/16 Pct Recovery = 94% Analysis Date = 11/17/16 Pct Recovery = 94% Analysis Date = 11/12/16 Pct Recovery = 94% Analysis Date = 11/12/16 Pct Recovery = 94% Analysis Date = 11/07/16 Pct Recovery = 94% Analysis Date = 11/07/16 Pct Recovery = 94% Analysis Date = 11/02/16 Pct Recovery = 94% Analysis Date = 11/02/16 Pct Recovery = 94% Analysis Date = 10/28/16 Pct Recovery = 94% Analysis Date = 10/28/16 Pct Recovery = 94% Analysis Date = 10/24/16 Pct Recovery = 94% Analysis Date = 10/24/16 Pct Recovery = 94% Analysis Date = 10/19/16 Pct Recovery = 94% Analysis Date = 10/19/16 Pct Recovery = 94% Analysis Date = 10/14/16 Pct Recovery = 94% Analysis Date = 10/14/16 Pct Recovery = 94% Analysis Date = 10/09/16 Pct Recovery = 94% Analysis Date = 10/09/16 Pct Recovery = 94% Analysis Date = 10/04/16 Pct Recovery = 94% Analysis Date = 10/04/16 Pct Recovery = 94% Analysis Date = 09/30/16 Pct Recovery = 94% Analysis Date = 09/30/16 Pct Recovery = 94% Analysis Date = 09/25/16 Pct Recovery = 94% Analysis Date = 09/25/16 Pct Recovery = 94% Analysis Date = 09/20/16 Pct Recovery = 94% Analysis Date = 09/20/16 Pct Recovery = 94% Analysis Date = 09/15/16 Pct Recovery = 94% Analysis Date = 09/15/16 Pct Recovery = 94% Analysis Date = 09/10/16 Pct Recovery = 94% Analysis Date = 09/10/16 Pct Recovery = 94% Analysis Date = 09/06/16 Pct Recovery = 94% Analysis Date = 09/06/16 Pct Recovery = 94% Analysis Date = 09/01/16 Pct Recovery = 94% Analysis Date = 09/01/16 Pct Recovery = 94% Analysis Date = 08/27/16 Pct Recovery = 93% Analysis Date = 08/27/16 Pct Recovery = 93% Analysis Date = 08/22/16 Pct Recovery = 93% Analysis Date = 08/22/16 Pct Recovery = 93% Analysis Date = 08/17/16 Pct Recovery = 93% Analysis Date = 08/17/16 Pct Recovery = 93% Analysis Date = 08/13/16 Pct Recovery = 93% Analysis Date = 08/13/16 Pct Recovery = 93% Analysis Date = 08/08/16 Pct Recovery = 93% Analysis Date = 08/08/16 Pct Recovery = 93% Analysis Date = 08/03/16 Pct Recovery = 93% Analysis Date = 08/03/16 Pct Recovery = 93% Analysis Date = 07/29/16 Pct Recovery = 93% Analysis Date = 07/29/16 Pct Recovery = 93% Analysis Date = 07/24/16 Pct Recovery = 93% Analysis Date = 07/24/16 Pct Recovery = 93% Analysis Date = 07/20/16 Pct Recovery = 93% Analysis Date = 07/20/16 Pct Recovery = 93% Analysis Date = 07/15/16 Pct Recovery = 93% Analysis Date = 07/15/16 Pct Recovery = 93% Analysis Date = 07/10/16 Pct Recovery = 93% Analysis Date = 07/10/16 Pct Recovery = 93% Analysis Date = 07/05/16 Pct Recovery = 93% Analysis Date = 07/05/16 Pct Recovery = 93% Analysis Date = 06/30/16 Pct Recovery = 93% Analysis Date = 06/30/16 Pct Recovery = 93% Analysis Date = 06/26/16 Pct Recovery = 93% Analysis Date = 06/26/16 Pct Recovery = 93% Analysis Date = 06/21/16 Pct Recovery = 93% Analysis Date = 06/21/16 Pct Recovery = 93% Analysis Date = 06/16/16 Pct Recovery = 93% Analysis Date = 06/16/16 Pct Recovery = 93% Analysis Date = 06/11/16 Pct Recovery = 93% Analysis Date = 06/11/16 Pct Recovery = 93% Analysis Date = 06/06/16 Pct Recovery = 93% Analysis Date = 06/06/16 Pct Recovery = 93% Analysis Date = 06/02/16 Pct Recovery = 93% Analysis Date = 06/02/16 Pct Recovery = 93% Analysis Date = 05/28/16 Pct Recovery = 93% Analysis Date = 05/28/16 Pct Recovery = 93% Analysis Date = 05/23/16 Pct Recovery = 93% Analysis Date = 05/23/16 Pct Recovery = 93% Analysis Date = 05/18/16 Pct Recovery = 92% Analysis Date = 05/18/16 Pct Recovery = 92% Analysis Date = 05/13/16 Pct Recovery = 92% Analysis Date = 05/13/16 Pct Recovery = 92% Analysis Date = 05/09/16 Pct Recovery = 92% Analysis Date = 05/09/16 Pct Recovery = 92% Analysis Date = 05/04/16 Pct Recovery = 92% Analysis Date = 05/04/16 Pct Recovery = 92% Analysis Date = 04/29/16 Pct Recovery = 92% Analysis Date = 04/29/16 Pct Recovery = 92% Analysis Date = 04/24/16 Pct Recovery = 92% Analysis Date = 04/24/16 Pct Recovery = 92% Analysis Date = 04/19/16 Pct Recovery = 92% Analysis Date = 04/19/16 Pct Recovery = 92% Analysis Date = 04/15/16 Pct Recovery = 92% Analysis Date = 04/15/16 Pct Recovery = 92% Analysis Date = 04/10/16 Pct Recovery = 92% Analysis Date = 04/10/16 Pct Recovery = 92% Analysis Date = 04/05/16 Pct Recovery = 92% Analysis Date = 04/05/16 Pct Recovery = 92% Analysis Date = 03/31/16 Pct Recovery = 92% Analysis Date = 03/31/16 Pct Recovery = 92% Analysis Date = 03/26/16 Pct Recovery = 92% Analysis Date = 03/26/16 Pct Recovery = 92% Analysis Date = 03/22/16 Pct Recovery = 92% Analysis Date = 03/22/16 Pct Recovery = 92% Analysis Date = 03/17/16 Pct Recovery = 92% Analysis Date = 03/17/16 Pct Recovery = 92% Analysis Date = 03/12/16 Pct Recovery = 92% Analysis Date = 03/12/16 Pct Recovery = 92% Analysis Date = 03/07/16 Pct Recovery = 92% Analysis Date = 03/07/16 Pct Recovery = 92% Analysis Date = 03/02/16 Pct Recovery = 92% Analysis Date = 03/02/16 Pct Recovery = 92% Analysis Date = 02/27/16 Pct Recovery = 92% Analysis Date = 02/27/16 Pct Recovery = 92% Analysis Date = 02/22/16 Pct Recovery = 92% Analysis Date = 02/22/16 Pct Recovery = 92% Analysis Date = 02/17/16 Pct Recovery = 92% Analysis Date = 02/17/16 Pct Recovery = 92% Analysis Date = 02/12/16 Pct Recovery = 92% Analysis Date = 02/12/16 Pct Recovery = 92% Analysis Date = 02/07/16 Pct Recovery = 92% Analysis Date = 02/07/16 Pct Recovery = 92% Analysis Date = 02/03/16 Pct Recovery = 92% Analysis Date = 02/03/16 Pct Recovery = 92% Analysis Date = 01/29/16 Pct Recovery = 92% Analysis Date = 01/29/16 Pct Recovery = 92% Analysis Date = 01/24/16 Pct Recovery = 92% Analysis Date = 01/24/16 Pct Recovery = 92% Analysis Date = 01/19/16 Pct Recovery = 92% Analysis Date = 01/19/16 Pct Recovery = 92% Analysis Date = 01/14/16 Pct Recovery = 92% Analysis Date = 01/14/16 Pct Recovery = 92% Analysis Date = 01/10/16 Pct Recovery = 92% Analysis Date = 01/10/16 Pct Recovery = 92% Analysis Date = 01/05/16 Pct Recovery = 92% Analysis Date = 01/05/16 Pct Recovery = 92% Analysis Date = 12/31/15 Pct Recovery = 92% Analysis Date = 12/31/15 Pct Recovery = 92% Analysis Date = 12/26/15 Pct Recovery = 92% Analysis Date = 12/26/15 Pct Recovery = 92% Analysis Date = 12/21/15 Pct Recovery = 92% Analysis Date = 12/21/15 Pct Recovery = 92% Analysis Date = 12/17/15 Pct Recovery = 92% Analysis Date = 12/17/15 Pct Recovery = 92% Analysis Date = 12/12/15 Pct Recovery = 92% Analysis Date = 12/12/15 Pct Recovery = 92% Analysis Date = 12/07/15 Pct Recovery = 92% Analysis Date = 12/07/15 Pct Recovery = 92% Analysis Date = 12/02/15 Pct Recovery = 92% Analysis Date = 12/02/15 Pct Recovery = 92% Analysis Date = 11/27/15 Pct Recovery = 92% Analysis Date = 11/27/15 Pct Recovery = 92% Analysis Date = 11/23/15 Pct Recovery = 92% Analysis Date = 11/23/15 Pct Recovery = 92% Analysis Date = 11/18/15 Pct Recovery = 92% Analysis Date = 11/18/15 Pct Recovery = 92% Analysis Date = 11/13/15 Pct Recovery = 92% Analysis Date = 11/13/15 Pct Recovery = 92% Analysis Date = 11/08/15 Pct Recovery = 92% Analysis Date = 11/08/15 Pct Recovery = 92% Analysis Date = 11/03/15 Pct Recovery = 92% Analysis Date = 11/03/15 Pct Recovery = 92% Analysis Date = 10/30/15 Pct Recovery = 92% Analysis Date = 10/30/15 Pct Recovery = 92% Analysis Date = 10/25/15 Pct Recovery = 92% Analysis Date = 10/25/15 Pct Recovery = 92% Analysis Date = 10/20/15 Pct Recovery = 92% Analysis Date = 10/20/15 Pct Recovery = 92% Analysis Date = 10/15/15 Pct Recovery = 92% Analysis Date = 10/15/15 Pct Recovery = 92% Analysis Date = 10/10/15 Pct Recovery = 92% Analysis Date = 10/10/15 Pct Recovery = 92% Analysis Date = 10/06/15 Pct Recovery = 92% Analysis Date = 10/06/15 Pct Recovery = 92% Analysis Date = 10/01/15 Pct Recovery = 92% Analysis Date = 10/01/15 Pct Recovery = 92% Analysis Date = 09/26/15 Pct Recovery = 92% Analysis Date = 09/26/15 Pct Recovery = 92% Analysis Date = 09/21/15 Pct Recovery = 92% Analysis Date = 09/21/15 Pct Recovery = 92% Analysis Date = 09/16/15 Pct Recovery = 92% Analysis Date = 09/16/15 Pct Recovery = 92% Analysis Date = 09/12/15 Pct Recovery = 92% Analysis Date = 09/12/15 Pct Recovery = 92% Analysis Date = 09/07/15 Pct Recovery = 92% Analysis Date = 09/07/15 Pct Recovery = 92% Analysis Date = 09/02/15 Pct Recovery = 92% Analysis Date = 09/02/15 Pct Recovery = 92% Analysis Date = 08/28/15 Pct Recovery = 92% Analysis Date = 08/28/15 Pct Recovery = 92% Analysis Date = 08/23/15 Pct Recovery = 91% Analysis Date = 08/23/15 Pct Recovery = 91% Analysis Date = 08/19/15 Pct Recovery = 91% Analysis Date = 08/19/15 Pct Recovery = 91% Analysis Date = 08/14/15 Pct Recovery = 91% Analysis Date = 08/14/15 Pct Recovery = 91% Analysis Date = 08/09/15 Pct Recovery = 91% Analysis Date = 08/09/15 Pct Recovery = 91% Analysis Date = 08/04/15 Pct Recovery = 91% Analysis Date = 08/04/15 Pct Recovery = 91% Analysis Date = 07/30/15 Pct Recovery = 91% Analysis Date = 07/30/15 Pct Recovery = 91% Analysis Date = 07/26/15 Pct Recovery = 91% Analysis Date = 07/26/15 Pct Recovery = 91% Analysis Date = 07/21/15 Pct Recovery = 91% Analysis Date = 07/21/15 Pct Recovery = 91% Analysis Date = 07/16/15 Pct Recovery = 91% Analysis Date = 07/16/15 Pct Recovery = 91% Analysis Date = 07/11/15 Pct Recovery = 91% Analysis Date = 07/11/15 Pct Recovery = 91% Analysis Date = 07/06/15 Pct Recovery = 91% Analysis Date = 07/06/15 Pct Recovery = 91% Analysis Date = 07/02/15 Pct Recovery = 91% Analysis Date = 07/02/15 Pct Recovery = 91% Analysis Date = 06/27/15 Pct Recovery = 91% Analysis Date = 06/27/15 Pct Recovery = 91% Analysis Date = 06/22/15 Pct Recovery = 91% Analysis Date = 06/22/15 Pct Recovery = 91% Analysis Date = 06/17/15 Pct Recovery = 91% Analysis Date = 06/17/15 Pct Recovery = 91% Analysis Date = 06/12/15 Pct Recovery = 91% Analysis Date = 06/12/15 Pct Recovery = 91% Analysis Date = 06/08/15 Pct Recovery = 91% Analysis Date = 06/08/15 Pct Recovery = 91% Analysis Date = 06/03/15 Pct Recovery = 91% Analysis Date = 06/03/15 Pct Recovery = 91% Analysis Date = 05/29/15 Pct Recovery = 91% Analysis Date = 05/29/15 Pct Recovery = 91% Analysis Date = 05/24/15 Pct Recovery = 91% Analysis Date = 05/24/15 Pct Recovery = 91% Analysis Date = 05/19/15 Pct Recovery = 91% Analysis Date = 05/19/15 Pct Recovery = 91% Analysis Date = 05/15/15 Pct Recovery = 91% Analysis Date = 05/15/15 Pct Recovery = 91% Analysis Date = 05/10/15 Pct Recovery = 91% Analysis Date = 05/10/15 Pct Recovery = 91% Analysis Date = 05/05/15 Pct Recovery = 91% Analysis Date = 05/05/15 Pct Recovery = 91% Analysis Date = 04/30/15 Pct Recovery = 91% Analysis Date = 04/30/15 Pct Recovery = 91% Analysis Date = 04/25/15 Pct Recovery = 91% Analysis Date = 04/25/15 Pct Recovery = 91% Analysis Date = 04/21/15 Pct Recovery = 91% Analysis Date = 04/21/15 Pct Recovery = 91% Analysis Date = 04/16/15 Pct Recovery = 91% Analysis Date = 04/16/15 Pct Recovery = 91% Analysis Date = 04/11/15 Pct Recovery = 91% Analysis Date = 04/11/15 Pct Recovery = 91% Analysis Date = 04/06/15 Pct Recovery = 91% Analysis Date = 04/06/15 Pct Recovery = 91% Analysis Date = 04/01/15 Pct Recovery = 91% Analysis Date = 04/01/15 Pct Recovery = 91% Analysis Date = 03/28/15 Pct Recovery = 91% Analysis Date = 03/28/15 Pct Recovery = 91% Analysis Date = 03/23/15 Pct Recovery = 91% Analysis Date = 03/23/15 Pct Recovery = 91% Analysis Date = 03/18/15 Pct Recovery = 91% Analysis Date = 03/18/15 Pct Recovery = 91% Analysis Date = 03/13/15 Pct Recovery = 91% Analysis Date = 03/13/15 Pct Recovery = 91% Analysis Date = 03/08/15 Pct Recovery = 91% Analysis Date = 03/08/15 Pct Recovery = 91% Analysis Date = 03/04/15 Pct Recovery = 91% Analysis Date = 03/04/15 Pct Recovery = 91% Analysis Date = 02/27/15 Pct Recovery = 91% Analysis Date = 02/27/15 Pct Recovery = 91% Analysis Date = 02/22/15 Pct Recovery = 91% Analysis Date = 02/22/15 Pct Recovery = 91% Analysis Date = 02/17/15 Pct Recovery = 91% Analysis Date = 02/17/15 Pct Recovery = 91% Analysis Date = 02/12/15 Pct Recovery = 91% Analysis Date = 02/12/15 Pct Recovery = 91% Analysis Date = 02/08/15 Pct Recovery = 91% Analysis Date = 02/08/15 Pct Recovery = 91% Analysis Date = 02/03/15 Pct Recovery = 91% Analysis Date = 02/03/15 Pct Recovery = 91% Analysis Date = 01/29/15 Pct Recovery = 91% Analysis Date = 01/29/15 Pct Recovery = 91% Analysis Date = 01/24/15 Pct Recovery = 91% Analysis Date = 01/24/15 Pct Recovery = 91% Analysis Date = 01/19/15 Pct Recovery = 91% Analysis Date = 01/19/15 Pct Recovery = 91% Analysis Date = 01/15/15 Pct Recovery = 91% Analysis Date = 01/15/15 Pct Recovery = 91% Analysis Date = 01/10/15 Pct Recovery = 91% Analysis Date = 01/10/15 Pct Recovery = 91% Analysis Date = 01/05/15 Pct Recovery = 91% Analysis Date = 01/05/15 Pct Recovery = 91% Analysis Date = 12/31/14 Pct Recovery = 91% Analysis Date = 12/31/14 Pct Recovery = 91% Analysis Date = 12/26/14 Pct Recovery = 91% Analysis Date = 12/26/14 Pct Recovery = 91% Analysis Date = 12/22/14 Pct Recovery = 91% Analysis Date = 12/22/14 Pct Recovery = 91% Analysis Date = 12/17/14 Pct Recovery = 91% Analysis Date = 12/17/14 Pct Recovery = 91% Analysis Date = 12/12/14 Pct Recovery = 91% Analysis Date = 12/12/14 Pct Recovery = 91% Analysis Date = 12/07/14 Pct Recovery = 91% Analysis Date = 12/07/14 Pct Recovery = 91% Analysis Date = 12/02/14 Pct Recovery = 91% Analysis Date = 12/02/14 Pct Recovery = 91% Analysis Date = 11/28/14 Pct Recovery = 91% Analysis Date = 11/28/14 Pct Recovery = 91% Analysis Date = 11/23/14 Pct Recovery = 91% Analysis Date = 11/23/14 Pct Recovery = 91% Analysis Date = 11/18/14 Pct Recovery = 91% Analysis Date = 11/18/14 Pct Recovery = 91% Analysis Date = 11/13/14 Pct Recovery = 91% Analysis Date = 11/13/14 Pct Recovery = 91% Analysis Date = 11/08/14 Pct Recovery = 91% Analysis Date = 11/08/14 Pct Recovery = 91% Analysis Date = 11/04/14 Pct Recovery = 91% Analysis Date = 11/04/14 Pct Recovery = 91% Analysis Date = 10/30/14 Pct Recovery = 91% Analysis Date = 10/30/14 Pct Recovery = 91% Analysis Date = 10/25/14 Pct Recovery = 91% Analysis Date = 10/25/14 Pct Recovery = 91% Analysis Date = 10/20/14 Pct Recovery = 91% Analysis Date = 10/20/14 Pct Recovery = 91% Analysis Date = 10/15/14 Pct Recovery = 91% Analysis Date = 10/15/14 Pct Recovery = 91% Analysis Date = 10/11/14 Pct Recovery = 91% Analysis Date = 10/11/14 Pct Recovery = 91% Analysis Date = 10/06/14 Pct Recovery = 91% Analysis Date = 10/06/14 Pct Recovery = 91% Analysis Date = 10/01/14 Pct Recovery = 91% Analysis Date = 10/01/14 Pct Recovery = 91% Analysis Date = 09/26/14 Pct Recovery = 91% Analysis Date = 09/26/14 Pct Recovery = 91% Analysis Date = 09/21/14 Pct Recovery = 91% Analysis Date = 09/21/14 Pct Recovery = 91% Analysis Date = 09/17/14 Pct Recovery = 91% Analysis Date = 09/17/14 Pct Recovery = 91% Analysis Date = 09/12/14 Pct Recovery = 91% Analysis Date = 09/12/14 Pct Recovery = 91% Analysis Date = 09/07/14 Pct Recovery = 91% Analysis Date = 09/07/14 Pct Recovery = 91% Analysis Date = 09/02/14 Pct Recovery = 91% Analysis Date = 09/02/14 Pct Recovery = 91% Analysis Date = 08/28/14 Pct Recovery = 91% Analysis Date = 08/28/14 Pct Recovery = 91% Analysis Date = 08/24/14 Pct Recovery = 91% Analysis Date = 08/24/14 Pct Recovery = 91% Analysis Date = 08/19/14 Pct Recovery = 91% Analysis Date = 08/19/14 Pct Recovery = 91% Analysis Date = 08/14/14 Pct Recovery = 91% Analysis Date = 08/14/14 Pct Recovery = 91% Analysis Date = 08/09/14 Pct Recovery = 91% Analysis Date = 08/09/14 Pct Recovery = 91% Analysis Date = 08/04/14 Pct Recovery = 91% Analysis Date = 08/04/14 Pct Recovery = 91% Analysis Date = 07/31/14 Pct Recovery = 91% Analysis Date = 07/31/14 Pct Recovery = 91% Analysis Date = 07/26/14 Pct Recovery = 91% Analysis Date = 07/26/14 Pct Recovery = 91% Analysis Date = 07/21/14 Pct Recovery = 91% Analysis Date = 07/21/14 Pct Recovery = 91% Analysis Date = 07/16/14 Pct Recovery = 91% Analysis Date = 07/16/14 Pct Recovery = 91% Analysis Date = 07/11/14 Pct Recovery = 91% Analysis Date = 07/11/14 Pct Recovery = 91% Analysis Date = 07/07/14 Pct Recovery = 91% Analysis Date = 07/07/14 Pct Recovery = 91% Analysis Date = 07/02/14 Pct Recovery = 91% Analysis Date = 07/02/14 Pct Recovery = 91% Analysis Date = 06/27/14 Pct Recovery = 91% Analysis Date = 06/27/14 Pct Recovery = 91% Analysis Date = 06/22/14 Pct Recovery = 91% Analysis Date = 06/22/14 Pct Recovery = 91% Analysis Date = 06/17/14 Pct Recovery = 91% Analysis Date = 06/17/14 Pct Recovery = 91% Analysis Date = 06/13/14 Pct Recovery = 91% Analysis Date = 06/13/14 Pct Recovery = 91% Analysis Date = 06/08/14 Pct Recovery = 91% Analysis Date = 06/08/14 Pct Recovery = 91% Analysis Date = 06/03/14 Pct Recovery = 91% Analysis Date = 06/03/14 Pct Recovery = 91% Analysis Date = 05/29/14 Pct Recovery = 91% Analysis Date = 05/29/14 Pct Recovery = 91% Analysis Date = 05/24/14 Pct Recovery = 91% Analysis Date = 05/24/14 Pct Recovery = 91% Analysis Date = 05/20/14 Pct Recovery = 91% Analysis Date = 05/20/14 Pct Recovery = 91% Analysis Date = 05/15/14 Pct Recovery = 91% Analysis Date = 05/15/14 Pct Recovery = 91% Analysis Date = 05/10/14 Pct Recovery = 91% Analysis Date = 05/10/14 Pct Recovery = 91% Analysis Date = 05/05/14 Pct Recovery = 91% Analysis Date = 05/05/14 Pct Recovery = 91% Analysis Date = 05/01/14 Pct Recovery = 91% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
1,1,2,2-TETRACHLOROETHANE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 49 92% 6% 92% 6%
Total 49 92% 6% 92% 6%

Sample Statistics
1,1,2,2-TETRACHLOROETHANE

Characteristic N % % Basis
Plotted 49 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 49 .  
False Negatives 0 0% 0 out of 49
Not Spiked 24 .  
False Positives 0 0% 0 out of 24

BQS OBSP Determination:
1,1,2-TRICHLOROETHANE
METHOD: 4440 , TESTIDCODE: 34511GCM66
Open Data Set

Analysis Date = 12/16/16 SpikeMix = NSI 041816AVOC: 40 µl & ChemService 5082900: 40 µl Pct Recovery = 110% Analysis Date = 08/04/16 SpikeMix = Crescent 03FF058: 40 µl & Supelco LC20141V: 40 µl Pct Recovery = 100% Analysis Date = 07/20/16 SpikeMix = Supelco LC20141V: 40 µl & Accu 216041125: 40 µl Pct Recovery = 92% Analysis Date = 04/09/15 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 94% Analysis Date = 08/19/14 SpikeMix = Spex Organics C1140417015: 20 µl & Accu 214031115: 20 µl Pct Recovery = 102% Analysis Date = 07/01/14 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 106% Analysis Date = 05/01/14 SpikeMix = Accu 214031115: 20 µl & NSI 032614: 20 µl Pct Recovery = 98% Analysis Date = 11/21/16 SpikeMix = Crescent 03FF058: 25 µl & Supelco LC20141V: 25 µl Pct Recovery = 99% Analysis Date = 09/08/16 SpikeMix = Supelco LC20141V: 25 µl & Accu 216041125: 25 µl Pct Recovery = 102% Analysis Date = 08/26/16 SpikeMix = NSI 041816AVOC: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 116% Analysis Date = 08/12/16 SpikeMix = ChemService 5082900: 25 µl & Phenova B20160319: 25 µl Pct Recovery = 107% Analysis Date = 06/30/16 SpikeMix = Crescent 03FF058: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 112% Analysis Date = 03/19/15 SpikeMix = Spex Organics C1140417015: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 102% Analysis Date = 12/17/14 SpikeMix = Supelco LC06438: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 96% Analysis Date = 11/14/14 SpikeMix = Crescent 03DD004: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 92% Analysis Date = 06/10/14 SpikeMix = Crescent 03DD004: 20 µl & NSI 032614: 20 µl Pct Recovery = 95% Analysis Date = 09/29/15 SpikeMix = Accu 215041380: 25 µl & ERA 0406-15-03: 25 µl Pct Recovery = 98% Analysis Date = 06/16/15 SpikeMix = ERA 0406-15-03: 25 µl & Supelco LC13545: 25 µl Pct Recovery = 93% Analysis Date = 07/13/15 SpikeMix = Crescent 04EE008: 25 µl & NSI 050515AVOC: 25 µl Pct Recovery = 101% Analysis Date = 11/29/16 SpikeMix = ChemService 5082900: 15 µl & Phenova B20160319: 15 µl Pct Recovery = 98% Analysis Date = 10/13/16 SpikeMix = NSI 041816AVOC: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 104% Analysis Date = 09/28/16 SpikeMix = Crescent 03FF058: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 109% Analysis Date = 06/30/16 SpikeMix = ChemService 5082900: 15 µl & Accu 216041125: 15 µl Pct Recovery = 100% Analysis Date = 06/10/16 SpikeMix = NSI 041816AVOC: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 109% Analysis Date = 05/27/16 SpikeMix = Phenova B20160319: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 103% Analysis Date = 04/26/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 117% Analysis Date = 03/04/16 SpikeMix = Accu 215041380: 15 µl & ERA 0406-15-03: 15 µl Pct Recovery = 89% Analysis Date = 02/05/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 99% Analysis Date = 10/16/15 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 99% Analysis Date = 11/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 93% Analysis Date = 10/17/15 SpikeMix = Crescent 04EE008: 15 µl & NSI 050515AVOC: 15 µl Pct Recovery = 100% Analysis Date = 06/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Accu 215041380: 15 µl Pct Recovery = 94% Analysis Date = 01/13/15 SpikeMix = Accu 214031115: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 102% Analysis Date = 09/09/14 SpikeMix = Accu 214031115: 10 µl & NSI 032614: 10 µl Pct Recovery = 103% Analysis Date = 07/23/14 SpikeMix = Spex Organics C1140417015: 10 µl & Accu 214031115: 10 µl Pct Recovery = 108% Analysis Date = 06/18/14 SpikeMix = Supelco LC06438: 10 µl & Accu 214031115: 10 µl Pct Recovery = 108% Analysis Date = 11/06/14 SpikeMix = Spex Organics C1140417015: 10 µl & Crescent 03DD004: 10 µl Pct Recovery = 96% Analysis Date = 10/04/14 SpikeMix = Crescent 03DD004: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 108% Analysis Date = 07/29/14 SpikeMix = Crescent 03DD004: 10 µl & NSI 032614: 10 µl Pct Recovery = 98% Analysis Date = 05/03/14 SpikeMix = Crescent 03DD004: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 93% Analysis Date = 11/20/15 SpikeMix = Accu 215041380: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 102% Analysis Date = 07/31/15 SpikeMix = Crescent 04EE008: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 87% Analysis Date = 06/27/15 SpikeMix = ERA 0406-15-03: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 100% Analysis Date = 03/17/16 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 94% Analysis Date = 01/27/16 SpikeMix = Crescent 04EE008: 10 µl & NSI 050515AVOC: 10 µl Pct Recovery = 98% Analysis Date = 12/10/15 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 102% Analysis Date = 09/03/15 SpikeMix = NSI 050515AVOC: 10 µl & Spex Organics EN150428007: 10 µl Pct Recovery = 100% Analysis Date = 12/15/16 Pct Recovery = 106% Analysis Date = 12/11/16 Pct Recovery = 106% Analysis Date = 12/11/16 Pct Recovery = 106% Analysis Date = 12/06/16 Pct Recovery = 106% Analysis Date = 12/06/16 Pct Recovery = 106% Analysis Date = 12/01/16 Pct Recovery = 106% Analysis Date = 12/01/16 Pct Recovery = 106% Analysis Date = 11/26/16 Pct Recovery = 106% Analysis Date = 11/26/16 Pct Recovery = 106% Analysis Date = 11/21/16 Pct Recovery = 105% Analysis Date = 11/21/16 Pct Recovery = 105% Analysis Date = 11/17/16 Pct Recovery = 105% Analysis Date = 11/17/16 Pct Recovery = 105% Analysis Date = 11/12/16 Pct Recovery = 105% Analysis Date = 11/12/16 Pct Recovery = 105% Analysis Date = 11/07/16 Pct Recovery = 105% Analysis Date = 11/07/16 Pct Recovery = 105% Analysis Date = 11/02/16 Pct Recovery = 105% Analysis Date = 11/02/16 Pct Recovery = 105% Analysis Date = 10/28/16 Pct Recovery = 105% Analysis Date = 10/28/16 Pct Recovery = 105% Analysis Date = 10/24/16 Pct Recovery = 105% Analysis Date = 10/24/16 Pct Recovery = 105% Analysis Date = 10/19/16 Pct Recovery = 105% Analysis Date = 10/19/16 Pct Recovery = 105% Analysis Date = 10/14/16 Pct Recovery = 105% Analysis Date = 10/14/16 Pct Recovery = 105% Analysis Date = 10/09/16 Pct Recovery = 105% Analysis Date = 10/09/16 Pct Recovery = 105% Analysis Date = 10/04/16 Pct Recovery = 105% Analysis Date = 10/04/16 Pct Recovery = 105% Analysis Date = 09/30/16 Pct Recovery = 105% Analysis Date = 09/30/16 Pct Recovery = 105% Analysis Date = 09/25/16 Pct Recovery = 105% Analysis Date = 09/25/16 Pct Recovery = 105% Analysis Date = 09/20/16 Pct Recovery = 104% Analysis Date = 09/20/16 Pct Recovery = 104% Analysis Date = 09/15/16 Pct Recovery = 104% Analysis Date = 09/15/16 Pct Recovery = 104% Analysis Date = 09/10/16 Pct Recovery = 104% Analysis Date = 09/10/16 Pct Recovery = 104% Analysis Date = 09/06/16 Pct Recovery = 104% Analysis Date = 09/06/16 Pct Recovery = 104% Analysis Date = 09/01/16 Pct Recovery = 104% Analysis Date = 09/01/16 Pct Recovery = 104% Analysis Date = 08/27/16 Pct Recovery = 104% Analysis Date = 08/27/16 Pct Recovery = 104% Analysis Date = 08/22/16 Pct Recovery = 104% Analysis Date = 08/22/16 Pct Recovery = 104% Analysis Date = 08/17/16 Pct Recovery = 104% Analysis Date = 08/17/16 Pct Recovery = 104% Analysis Date = 08/13/16 Pct Recovery = 104% Analysis Date = 08/13/16 Pct Recovery = 104% Analysis Date = 08/08/16 Pct Recovery = 104% Analysis Date = 08/08/16 Pct Recovery = 104% Analysis Date = 08/03/16 Pct Recovery = 104% Analysis Date = 08/03/16 Pct Recovery = 104% Analysis Date = 07/29/16 Pct Recovery = 104% Analysis Date = 07/29/16 Pct Recovery = 104% Analysis Date = 07/24/16 Pct Recovery = 104% Analysis Date = 07/24/16 Pct Recovery = 104% Analysis Date = 07/20/16 Pct Recovery = 103% Analysis Date = 07/20/16 Pct Recovery = 103% Analysis Date = 07/15/16 Pct Recovery = 103% Analysis Date = 07/15/16 Pct Recovery = 103% Analysis Date = 07/10/16 Pct Recovery = 103% Analysis Date = 07/10/16 Pct Recovery = 103% Analysis Date = 07/05/16 Pct Recovery = 103% Analysis Date = 07/05/16 Pct Recovery = 103% Analysis Date = 06/30/16 Pct Recovery = 103% Analysis Date = 06/30/16 Pct Recovery = 103% Analysis Date = 06/26/16 Pct Recovery = 103% Analysis Date = 06/26/16 Pct Recovery = 103% Analysis Date = 06/21/16 Pct Recovery = 103% Analysis Date = 06/21/16 Pct Recovery = 103% Analysis Date = 06/16/16 Pct Recovery = 103% Analysis Date = 06/16/16 Pct Recovery = 103% Analysis Date = 06/11/16 Pct Recovery = 103% Analysis Date = 06/11/16 Pct Recovery = 103% Analysis Date = 06/06/16 Pct Recovery = 103% Analysis Date = 06/06/16 Pct Recovery = 103% Analysis Date = 06/02/16 Pct Recovery = 103% Analysis Date = 06/02/16 Pct Recovery = 103% Analysis Date = 05/28/16 Pct Recovery = 103% Analysis Date = 05/28/16 Pct Recovery = 103% Analysis Date = 05/23/16 Pct Recovery = 102% Analysis Date = 05/23/16 Pct Recovery = 102% Analysis Date = 05/18/16 Pct Recovery = 102% Analysis Date = 05/18/16 Pct Recovery = 102% Analysis Date = 05/13/16 Pct Recovery = 102% Analysis Date = 05/13/16 Pct Recovery = 102% Analysis Date = 05/09/16 Pct Recovery = 102% Analysis Date = 05/09/16 Pct Recovery = 102% Analysis Date = 05/04/16 Pct Recovery = 102% Analysis Date = 05/04/16 Pct Recovery = 102% Analysis Date = 04/29/16 Pct Recovery = 102% Analysis Date = 04/29/16 Pct Recovery = 102% Analysis Date = 04/24/16 Pct Recovery = 102% Analysis Date = 04/24/16 Pct Recovery = 102% Analysis Date = 04/19/16 Pct Recovery = 102% Analysis Date = 04/19/16 Pct Recovery = 102% Analysis Date = 04/15/16 Pct Recovery = 102% Analysis Date = 04/15/16 Pct Recovery = 102% Analysis Date = 04/10/16 Pct Recovery = 102% Analysis Date = 04/10/16 Pct Recovery = 102% Analysis Date = 04/05/16 Pct Recovery = 101% Analysis Date = 04/05/16 Pct Recovery = 101% Analysis Date = 03/31/16 Pct Recovery = 101% Analysis Date = 03/31/16 Pct Recovery = 101% Analysis Date = 03/26/16 Pct Recovery = 101% Analysis Date = 03/26/16 Pct Recovery = 101% Analysis Date = 03/22/16 Pct Recovery = 101% Analysis Date = 03/22/16 Pct Recovery = 101% Analysis Date = 03/17/16 Pct Recovery = 101% Analysis Date = 03/17/16 Pct Recovery = 101% Analysis Date = 03/12/16 Pct Recovery = 101% Analysis Date = 03/12/16 Pct Recovery = 101% Analysis Date = 03/07/16 Pct Recovery = 101% Analysis Date = 03/07/16 Pct Recovery = 101% Analysis Date = 03/02/16 Pct Recovery = 101% Analysis Date = 03/02/16 Pct Recovery = 101% Analysis Date = 02/27/16 Pct Recovery = 101% Analysis Date = 02/27/16 Pct Recovery = 101% Analysis Date = 02/22/16 Pct Recovery = 101% Analysis Date = 02/22/16 Pct Recovery = 101% Analysis Date = 02/17/16 Pct Recovery = 100% Analysis Date = 02/17/16 Pct Recovery = 100% Analysis Date = 02/12/16 Pct Recovery = 100% Analysis Date = 02/12/16 Pct Recovery = 100% Analysis Date = 02/07/16 Pct Recovery = 100% Analysis Date = 02/07/16 Pct Recovery = 100% Analysis Date = 02/03/16 Pct Recovery = 100% Analysis Date = 02/03/16 Pct Recovery = 100% Analysis Date = 01/29/16 Pct Recovery = 100% Analysis Date = 01/29/16 Pct Recovery = 100% Analysis Date = 01/24/16 Pct Recovery = 100% Analysis Date = 01/24/16 Pct Recovery = 100% Analysis Date = 01/19/16 Pct Recovery = 100% Analysis Date = 01/19/16 Pct Recovery = 100% Analysis Date = 01/14/16 Pct Recovery = 100% Analysis Date = 01/14/16 Pct Recovery = 100% Analysis Date = 01/10/16 Pct Recovery = 100% Analysis Date = 01/10/16 Pct Recovery = 100% Analysis Date = 01/05/16 Pct Recovery = 99% Analysis Date = 01/05/16 Pct Recovery = 99% Analysis Date = 12/31/15 Pct Recovery = 99% Analysis Date = 12/31/15 Pct Recovery = 99% Analysis Date = 12/26/15 Pct Recovery = 99% Analysis Date = 12/26/15 Pct Recovery = 99% Analysis Date = 12/21/15 Pct Recovery = 99% Analysis Date = 12/21/15 Pct Recovery = 99% Analysis Date = 12/17/15 Pct Recovery = 99% Analysis Date = 12/17/15 Pct Recovery = 99% Analysis Date = 12/12/15 Pct Recovery = 99% Analysis Date = 12/12/15 Pct Recovery = 99% Analysis Date = 12/07/15 Pct Recovery = 99% Analysis Date = 12/07/15 Pct Recovery = 99% Analysis Date = 12/02/15 Pct Recovery = 99% Analysis Date = 12/02/15 Pct Recovery = 99% Analysis Date = 11/27/15 Pct Recovery = 99% Analysis Date = 11/27/15 Pct Recovery = 99% Analysis Date = 11/23/15 Pct Recovery = 98% Analysis Date = 11/23/15 Pct Recovery = 98% Analysis Date = 11/18/15 Pct Recovery = 98% Analysis Date = 11/18/15 Pct Recovery = 98% Analysis Date = 11/13/15 Pct Recovery = 98% Analysis Date = 11/13/15 Pct Recovery = 98% Analysis Date = 11/08/15 Pct Recovery = 98% Analysis Date = 11/08/15 Pct Recovery = 98% Analysis Date = 11/03/15 Pct Recovery = 98% Analysis Date = 11/03/15 Pct Recovery = 98% Analysis Date = 10/30/15 Pct Recovery = 98% Analysis Date = 10/30/15 Pct Recovery = 98% Analysis Date = 10/25/15 Pct Recovery = 98% Analysis Date = 10/25/15 Pct Recovery = 98% Analysis Date = 10/20/15 Pct Recovery = 98% Analysis Date = 10/20/15 Pct Recovery = 98% Analysis Date = 10/15/15 Pct Recovery = 98% Analysis Date = 10/15/15 Pct Recovery = 98% Analysis Date = 10/10/15 Pct Recovery = 98% Analysis Date = 10/10/15 Pct Recovery = 98% Analysis Date = 10/06/15 Pct Recovery = 98% Analysis Date = 10/06/15 Pct Recovery = 98% Analysis Date = 10/01/15 Pct Recovery = 98% Analysis Date = 10/01/15 Pct Recovery = 98% Analysis Date = 09/26/15 Pct Recovery = 98% Analysis Date = 09/26/15 Pct Recovery = 98% Analysis Date = 09/21/15 Pct Recovery = 98% Analysis Date = 09/21/15 Pct Recovery = 98% Analysis Date = 09/16/15 Pct Recovery = 98% Analysis Date = 09/16/15 Pct Recovery = 98% Analysis Date = 09/12/15 Pct Recovery = 98% Analysis Date = 09/12/15 Pct Recovery = 98% Analysis Date = 09/07/15 Pct Recovery = 98% Analysis Date = 09/07/15 Pct Recovery = 98% Analysis Date = 09/02/15 Pct Recovery = 98% Analysis Date = 09/02/15 Pct Recovery = 98% Analysis Date = 08/28/15 Pct Recovery = 97% Analysis Date = 08/28/15 Pct Recovery = 97% Analysis Date = 08/23/15 Pct Recovery = 97% Analysis Date = 08/23/15 Pct Recovery = 97% Analysis Date = 08/19/15 Pct Recovery = 97% Analysis Date = 08/19/15 Pct Recovery = 97% Analysis Date = 08/14/15 Pct Recovery = 97% Analysis Date = 08/14/15 Pct Recovery = 97% Analysis Date = 08/09/15 Pct Recovery = 97% Analysis Date = 08/09/15 Pct Recovery = 97% Analysis Date = 08/04/15 Pct Recovery = 97% Analysis Date = 08/04/15 Pct Recovery = 97% Analysis Date = 07/30/15 Pct Recovery = 97% Analysis Date = 07/30/15 Pct Recovery = 97% Analysis Date = 07/26/15 Pct Recovery = 97% Analysis Date = 07/26/15 Pct Recovery = 97% Analysis Date = 07/21/15 Pct Recovery = 97% Analysis Date = 07/21/15 Pct Recovery = 97% Analysis Date = 07/16/15 Pct Recovery = 97% Analysis Date = 07/16/15 Pct Recovery = 97% Analysis Date = 07/11/15 Pct Recovery = 97% Analysis Date = 07/11/15 Pct Recovery = 97% Analysis Date = 07/06/15 Pct Recovery = 97% Analysis Date = 07/06/15 Pct Recovery = 97% Analysis Date = 07/02/15 Pct Recovery = 97% Analysis Date = 07/02/15 Pct Recovery = 97% Analysis Date = 06/27/15 Pct Recovery = 97% Analysis Date = 06/27/15 Pct Recovery = 97% Analysis Date = 06/22/15 Pct Recovery = 97% Analysis Date = 06/22/15 Pct Recovery = 97% Analysis Date = 06/17/15 Pct Recovery = 97% Analysis Date = 06/17/15 Pct Recovery = 97% Analysis Date = 06/12/15 Pct Recovery = 97% Analysis Date = 06/12/15 Pct Recovery = 97% Analysis Date = 06/08/15 Pct Recovery = 97% Analysis Date = 06/08/15 Pct Recovery = 97% Analysis Date = 06/03/15 Pct Recovery = 97% Analysis Date = 06/03/15 Pct Recovery = 97% Analysis Date = 05/29/15 Pct Recovery = 97% Analysis Date = 05/29/15 Pct Recovery = 97% Analysis Date = 05/24/15 Pct Recovery = 97% Analysis Date = 05/24/15 Pct Recovery = 97% Analysis Date = 05/19/15 Pct Recovery = 98% Analysis Date = 05/19/15 Pct Recovery = 98% Analysis Date = 05/15/15 Pct Recovery = 98% Analysis Date = 05/15/15 Pct Recovery = 98% Analysis Date = 05/10/15 Pct Recovery = 98% Analysis Date = 05/10/15 Pct Recovery = 98% Analysis Date = 05/05/15 Pct Recovery = 98% Analysis Date = 05/05/15 Pct Recovery = 98% Analysis Date = 04/30/15 Pct Recovery = 98% Analysis Date = 04/30/15 Pct Recovery = 98% Analysis Date = 04/25/15 Pct Recovery = 98% Analysis Date = 04/25/15 Pct Recovery = 98% Analysis Date = 04/21/15 Pct Recovery = 98% Analysis Date = 04/21/15 Pct Recovery = 98% Analysis Date = 04/16/15 Pct Recovery = 98% Analysis Date = 04/16/15 Pct Recovery = 98% Analysis Date = 04/11/15 Pct Recovery = 98% Analysis Date = 04/11/15 Pct Recovery = 98% Analysis Date = 04/06/15 Pct Recovery = 98% Analysis Date = 04/06/15 Pct Recovery = 98% Analysis Date = 04/01/15 Pct Recovery = 98% Analysis Date = 04/01/15 Pct Recovery = 98% Analysis Date = 03/28/15 Pct Recovery = 98% Analysis Date = 03/28/15 Pct Recovery = 98% Analysis Date = 03/23/15 Pct Recovery = 98% Analysis Date = 03/23/15 Pct Recovery = 98% Analysis Date = 03/18/15 Pct Recovery = 98% Analysis Date = 03/18/15 Pct Recovery = 98% Analysis Date = 03/13/15 Pct Recovery = 98% Analysis Date = 03/13/15 Pct Recovery = 98% Analysis Date = 03/08/15 Pct Recovery = 98% Analysis Date = 03/08/15 Pct Recovery = 98% Analysis Date = 03/04/15 Pct Recovery = 98% Analysis Date = 03/04/15 Pct Recovery = 98% Analysis Date = 02/27/15 Pct Recovery = 98% Analysis Date = 02/27/15 Pct Recovery = 98% Analysis Date = 02/22/15 Pct Recovery = 98% Analysis Date = 02/22/15 Pct Recovery = 98% Analysis Date = 02/17/15 Pct Recovery = 98% Analysis Date = 02/17/15 Pct Recovery = 98% Analysis Date = 02/12/15 Pct Recovery = 98% Analysis Date = 02/12/15 Pct Recovery = 98% Analysis Date = 02/08/15 Pct Recovery = 98% Analysis Date = 02/08/15 Pct Recovery = 98% Analysis Date = 02/03/15 Pct Recovery = 98% Analysis Date = 02/03/15 Pct Recovery = 98% Analysis Date = 01/29/15 Pct Recovery = 99% Analysis Date = 01/29/15 Pct Recovery = 99% Analysis Date = 01/24/15 Pct Recovery = 99% Analysis Date = 01/24/15 Pct Recovery = 99% Analysis Date = 01/19/15 Pct Recovery = 99% Analysis Date = 01/19/15 Pct Recovery = 99% Analysis Date = 01/15/15 Pct Recovery = 99% Analysis Date = 01/15/15 Pct Recovery = 99% Analysis Date = 01/10/15 Pct Recovery = 99% Analysis Date = 01/10/15 Pct Recovery = 99% Analysis Date = 01/05/15 Pct Recovery = 99% Analysis Date = 01/05/15 Pct Recovery = 99% Analysis Date = 12/31/14 Pct Recovery = 99% Analysis Date = 12/31/14 Pct Recovery = 99% Analysis Date = 12/26/14 Pct Recovery = 99% Analysis Date = 12/26/14 Pct Recovery = 99% Analysis Date = 12/22/14 Pct Recovery = 99% Analysis Date = 12/22/14 Pct Recovery = 99% Analysis Date = 12/17/14 Pct Recovery = 99% Analysis Date = 12/17/14 Pct Recovery = 99% Analysis Date = 12/12/14 Pct Recovery = 99% Analysis Date = 12/12/14 Pct Recovery = 99% Analysis Date = 12/07/14 Pct Recovery = 99% Analysis Date = 12/07/14 Pct Recovery = 99% Analysis Date = 12/02/14 Pct Recovery = 99% Analysis Date = 12/02/14 Pct Recovery = 99% Analysis Date = 11/28/14 Pct Recovery = 99% Analysis Date = 11/28/14 Pct Recovery = 99% Analysis Date = 11/23/14 Pct Recovery = 99% Analysis Date = 11/23/14 Pct Recovery = 99% Analysis Date = 11/18/14 Pct Recovery = 99% Analysis Date = 11/18/14 Pct Recovery = 99% Analysis Date = 11/13/14 Pct Recovery = 99% Analysis Date = 11/13/14 Pct Recovery = 99% Analysis Date = 11/08/14 Pct Recovery = 100% Analysis Date = 11/08/14 Pct Recovery = 100% Analysis Date = 11/04/14 Pct Recovery = 100% Analysis Date = 11/04/14 Pct Recovery = 100% Analysis Date = 10/30/14 Pct Recovery = 100% Analysis Date = 10/30/14 Pct Recovery = 100% Analysis Date = 10/25/14 Pct Recovery = 100% Analysis Date = 10/25/14 Pct Recovery = 100% Analysis Date = 10/20/14 Pct Recovery = 100% Analysis Date = 10/20/14 Pct Recovery = 100% Analysis Date = 10/15/14 Pct Recovery = 100% Analysis Date = 10/15/14 Pct Recovery = 100% Analysis Date = 10/11/14 Pct Recovery = 100% Analysis Date = 10/11/14 Pct Recovery = 100% Analysis Date = 10/06/14 Pct Recovery = 100% Analysis Date = 10/06/14 Pct Recovery = 100% Analysis Date = 10/01/14 Pct Recovery = 100% Analysis Date = 10/01/14 Pct Recovery = 100% Analysis Date = 09/26/14 Pct Recovery = 100% Analysis Date = 09/26/14 Pct Recovery = 100% Analysis Date = 09/21/14 Pct Recovery = 100% Analysis Date = 09/21/14 Pct Recovery = 100% Analysis Date = 09/17/14 Pct Recovery = 100% Analysis Date = 09/17/14 Pct Recovery = 100% Analysis Date = 09/12/14 Pct Recovery = 100% Analysis Date = 09/12/14 Pct Recovery = 100% Analysis Date = 09/07/14 Pct Recovery = 100% Analysis Date = 09/07/14 Pct Recovery = 100% Analysis Date = 09/02/14 Pct Recovery = 100% Analysis Date = 09/02/14 Pct Recovery = 100% Analysis Date = 08/28/14 Pct Recovery = 100% Analysis Date = 08/28/14 Pct Recovery = 100% Analysis Date = 08/24/14 Pct Recovery = 100% Analysis Date = 08/24/14 Pct Recovery = 100% Analysis Date = 08/19/14 Pct Recovery = 100% Analysis Date = 08/19/14 Pct Recovery = 100% Analysis Date = 08/14/14 Pct Recovery = 100% Analysis Date = 08/14/14 Pct Recovery = 100% Analysis Date = 08/09/14 Pct Recovery = 100% Analysis Date = 08/09/14 Pct Recovery = 100% Analysis Date = 08/04/14 Pct Recovery = 100% Analysis Date = 08/04/14 Pct Recovery = 100% Analysis Date = 07/31/14 Pct Recovery = 101% Analysis Date = 07/31/14 Pct Recovery = 101% Analysis Date = 07/26/14 Pct Recovery = 101% Analysis Date = 07/26/14 Pct Recovery = 101% Analysis Date = 07/21/14 Pct Recovery = 101% Analysis Date = 07/21/14 Pct Recovery = 101% Analysis Date = 07/16/14 Pct Recovery = 101% Analysis Date = 07/16/14 Pct Recovery = 101% Analysis Date = 07/11/14 Pct Recovery = 101% Analysis Date = 07/11/14 Pct Recovery = 101% Analysis Date = 07/07/14 Pct Recovery = 101% Analysis Date = 07/07/14 Pct Recovery = 101% Analysis Date = 07/02/14 Pct Recovery = 101% Analysis Date = 07/02/14 Pct Recovery = 101% Analysis Date = 06/27/14 Pct Recovery = 101% Analysis Date = 06/27/14 Pct Recovery = 101% Analysis Date = 06/22/14 Pct Recovery = 101% Analysis Date = 06/22/14 Pct Recovery = 101% Analysis Date = 06/17/14 Pct Recovery = 101% Analysis Date = 06/17/14 Pct Recovery = 101% Analysis Date = 06/13/14 Pct Recovery = 101% Analysis Date = 06/13/14 Pct Recovery = 101% Analysis Date = 06/08/14 Pct Recovery = 101% Analysis Date = 06/08/14 Pct Recovery = 101% Analysis Date = 06/03/14 Pct Recovery = 101% Analysis Date = 06/03/14 Pct Recovery = 101% Analysis Date = 05/29/14 Pct Recovery = 101% Analysis Date = 05/29/14 Pct Recovery = 101% Analysis Date = 05/24/14 Pct Recovery = 101% Analysis Date = 05/24/14 Pct Recovery = 101% Analysis Date = 05/20/14 Pct Recovery = 101% Analysis Date = 05/20/14 Pct Recovery = 101% Analysis Date = 05/15/14 Pct Recovery = 101% Analysis Date = 05/15/14 Pct Recovery = 101% Analysis Date = 05/10/14 Pct Recovery = 101% Analysis Date = 05/10/14 Pct Recovery = 101% Analysis Date = 05/05/14 Pct Recovery = 101% Analysis Date = 05/05/14 Pct Recovery = 101% Analysis Date = 05/01/14 Pct Recovery = 101% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
1,1,2-TRICHLOROETHANE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 47 101% 7% 100% 6%
Total 47 101% 7% 100% 6%

Sample Statistics
1,1,2-TRICHLOROETHANE

Characteristic N % % Basis
Plotted 47 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 47 .  
False Negatives 0 0% 0 out of 47
Not Spiked 26 .  
False Positives 1 4% 1 out of 26

BQS OBSP Determination:
1,1,2-TRICHLOROTRIFLUOROETHANE
METHOD: 4440 , TESTIDCODE: 77652GCM66
Open Data Set

Analysis Date = 12/16/16 SpikeMix = NSI 041816AVOC: 40 µl & ChemService 5082900: 40 µl Pct Recovery = 94% Analysis Date = 12/12/16 SpikeMix = Accu 216041125: 40 µl & Crescent 03FF058: 40 µl Pct Recovery = 88% Analysis Date = 08/04/16 SpikeMix = Crescent 03FF058: 40 µl & Supelco LC20141V: 40 µl Pct Recovery = 99% Analysis Date = 07/14/16 SpikeMix = Accu 216041125: 40 µl & NSI 041816AVOC: 40 µl Pct Recovery = 99% Analysis Date = 11/21/16 SpikeMix = Crescent 03FF058: 25 µl & Supelco LC20141V: 25 µl Pct Recovery = 77% Analysis Date = 08/26/16 SpikeMix = NSI 041816AVOC: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 106% Analysis Date = 06/30/16 SpikeMix = Crescent 03FF058: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 95% Analysis Date = 06/21/16 SpikeMix = Phenova B20160319: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 86% Analysis Date = 05/24/16 SpikeMix = Accu 216041125: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 91% Analysis Date = 11/22/14 SpikeMix = NSI 032614: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 151% Analysis Date = 06/10/14 SpikeMix = Crescent 03DD004: 20 µl & NSI 032614: 20 µl Pct Recovery = 135% Analysis Date = 06/10/14 SpikeMix = NSI 032614: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 144% Analysis Date = 05/01/14 SpikeMix = Accu 214031115: 20 µl & NSI 032614: 20 µl Pct Recovery = 135% Analysis Date = 04/09/15 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 109% Analysis Date = 03/06/15 SpikeMix = ERA 0227-14-06.1A: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 101% Analysis Date = 11/14/14 SpikeMix = Crescent 03DD004: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 99% Analysis Date = 08/16/14 SpikeMix = ERA 0227-14-06.1A: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 114% Analysis Date = 07/01/14 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 119% Analysis Date = 07/13/15 SpikeMix = Crescent 04EE008: 25 µl & NSI 050515AVOC: 25 µl Pct Recovery = 114% Analysis Date = 09/29/15 SpikeMix = Accu 215041380: 25 µl & ERA 0406-15-03: 25 µl Pct Recovery = 93% Analysis Date = 06/16/15 SpikeMix = ERA 0406-15-03: 25 µl & Supelco LC13545: 25 µl Pct Recovery = 90% Analysis Date = 10/13/16 SpikeMix = Accu 216041125: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 102% Analysis Date = 10/13/16 SpikeMix = NSI 041816AVOC: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 94% Analysis Date = 09/28/16 SpikeMix = Crescent 03FF058: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 99% Analysis Date = 09/08/16 SpikeMix = Phenova B20160319: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 93% Analysis Date = 08/20/16 SpikeMix = Accu 216041125: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 101% Analysis Date = 07/29/16 SpikeMix = Phenova B20160319: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 97% Analysis Date = 06/10/16 SpikeMix = NSI 041816AVOC: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 93% Analysis Date = 11/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 99% Analysis Date = 10/17/15 SpikeMix = Crescent 04EE008: 15 µl & NSI 050515AVOC: 15 µl Pct Recovery = 106% Analysis Date = 06/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Accu 215041380: 15 µl Pct Recovery = 140% Analysis Date = 04/26/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 83% Analysis Date = 03/04/16 SpikeMix = Accu 215041380: 15 µl & ERA 0406-15-03: 15 µl Pct Recovery = 76% Analysis Date = 02/05/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 88% Analysis Date = 10/16/15 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 84% Analysis Date = 09/09/14 SpikeMix = Accu 214031115: 10 µl & NSI 032614: 10 µl Pct Recovery = 139% Analysis Date = 09/09/14 SpikeMix = NSI 032614: 10 µl & Spex Organics C1140417015: 10 µl Pct Recovery = 143% Analysis Date = 07/29/14 SpikeMix = Crescent 03DD004: 10 µl & NSI 032614: 10 µl Pct Recovery = 149% Analysis Date = 05/30/14 SpikeMix = NSI 032614: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 126% Analysis Date = 01/13/15 SpikeMix = Accu 214031115: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 88% Analysis Date = 10/21/14 SpikeMix = ERA 0227-14-06.1A: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 106% Analysis Date = 10/04/14 SpikeMix = Crescent 03DD004: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 121% Analysis Date = 07/11/14 SpikeMix = Spex Organics C1140417015: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 92% Analysis Date = 03/17/16 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 105% Analysis Date = 01/27/16 SpikeMix = Crescent 04EE008: 10 µl & NSI 050515AVOC: 10 µl Pct Recovery = 111% Analysis Date = 12/10/15 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 122% Analysis Date = 09/03/15 SpikeMix = NSI 050515AVOC: 10 µl & Spex Organics EN150428007: 10 µl Pct Recovery = 127% Analysis Date = 11/20/15 SpikeMix = Accu 215041380: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 96% Analysis Date = 07/31/15 SpikeMix = Crescent 04EE008: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 88% Analysis Date = 06/27/15 SpikeMix = ERA 0406-15-03: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 93% Analysis Date = 12/15/16 Pct Recovery = 93% Analysis Date = 12/11/16 Pct Recovery = 93% Analysis Date = 12/11/16 Pct Recovery = 93% Analysis Date = 12/06/16 Pct Recovery = 93% Analysis Date = 12/06/16 Pct Recovery = 93% Analysis Date = 12/01/16 Pct Recovery = 93% Analysis Date = 12/01/16 Pct Recovery = 93% Analysis Date = 11/26/16 Pct Recovery = 93% Analysis Date = 11/26/16 Pct Recovery = 93% Analysis Date = 11/21/16 Pct Recovery = 93% Analysis Date = 11/21/16 Pct Recovery = 93% Analysis Date = 11/17/16 Pct Recovery = 93% Analysis Date = 11/17/16 Pct Recovery = 93% Analysis Date = 11/12/16 Pct Recovery = 93% Analysis Date = 11/12/16 Pct Recovery = 93% Analysis Date = 11/07/16 Pct Recovery = 93% Analysis Date = 11/07/16 Pct Recovery = 93% Analysis Date = 11/02/16 Pct Recovery = 93% Analysis Date = 11/02/16 Pct Recovery = 93% Analysis Date = 10/28/16 Pct Recovery = 93% Analysis Date = 10/28/16 Pct Recovery = 93% Analysis Date = 10/24/16 Pct Recovery = 93% Analysis Date = 10/24/16 Pct Recovery = 93% Analysis Date = 10/19/16 Pct Recovery = 93% Analysis Date = 10/19/16 Pct Recovery = 93% Analysis Date = 10/14/16 Pct Recovery = 93% Analysis Date = 10/14/16 Pct Recovery = 93% Analysis Date = 10/09/16 Pct Recovery = 94% Analysis Date = 10/09/16 Pct Recovery = 94% Analysis Date = 10/04/16 Pct Recovery = 94% Analysis Date = 10/04/16 Pct Recovery = 94% Analysis Date = 09/30/16 Pct Recovery = 94% Analysis Date = 09/30/16 Pct Recovery = 94% Analysis Date = 09/25/16 Pct Recovery = 94% Analysis Date = 09/25/16 Pct Recovery = 94% Analysis Date = 09/20/16 Pct Recovery = 94% Analysis Date = 09/20/16 Pct Recovery = 94% Analysis Date = 09/15/16 Pct Recovery = 94% Analysis Date = 09/15/16 Pct Recovery = 94% Analysis Date = 09/10/16 Pct Recovery = 94% Analysis Date = 09/10/16 Pct Recovery = 94% Analysis Date = 09/06/16 Pct Recovery = 94% Analysis Date = 09/06/16 Pct Recovery = 94% Analysis Date = 09/01/16 Pct Recovery = 94% Analysis Date = 09/01/16 Pct Recovery = 94% Analysis Date = 08/27/16 Pct Recovery = 94% Analysis Date = 08/27/16 Pct Recovery = 94% Analysis Date = 08/22/16 Pct Recovery = 94% Analysis Date = 08/22/16 Pct Recovery = 94% Analysis Date = 08/17/16 Pct Recovery = 94% Analysis Date = 08/17/16 Pct Recovery = 94% Analysis Date = 08/13/16 Pct Recovery = 94% Analysis Date = 08/13/16 Pct Recovery = 94% Analysis Date = 08/08/16 Pct Recovery = 94% Analysis Date = 08/08/16 Pct Recovery = 94% Analysis Date = 08/03/16 Pct Recovery = 95% Analysis Date = 08/03/16 Pct Recovery = 95% Analysis Date = 07/29/16 Pct Recovery = 95% Analysis Date = 07/29/16 Pct Recovery = 95% Analysis Date = 07/24/16 Pct Recovery = 95% Analysis Date = 07/24/16 Pct Recovery = 95% Analysis Date = 07/20/16 Pct Recovery = 95% Analysis Date = 07/20/16 Pct Recovery = 95% Analysis Date = 07/15/16 Pct Recovery = 95% Analysis Date = 07/15/16 Pct Recovery = 95% Analysis Date = 07/10/16 Pct Recovery = 95% Analysis Date = 07/10/16 Pct Recovery = 95% Analysis Date = 07/05/16 Pct Recovery = 95% Analysis Date = 07/05/16 Pct Recovery = 95% Analysis Date = 06/30/16 Pct Recovery = 95% Analysis Date = 06/30/16 Pct Recovery = 95% Analysis Date = 06/26/16 Pct Recovery = 95% Analysis Date = 06/26/16 Pct Recovery = 95% Analysis Date = 06/21/16 Pct Recovery = 95% Analysis Date = 06/21/16 Pct Recovery = 95% Analysis Date = 06/16/16 Pct Recovery = 95% Analysis Date = 06/16/16 Pct Recovery = 95% Analysis Date = 06/11/16 Pct Recovery = 95% Analysis Date = 06/11/16 Pct Recovery = 95% Analysis Date = 06/06/16 Pct Recovery = 95% Analysis Date = 06/06/16 Pct Recovery = 95% Analysis Date = 06/02/16 Pct Recovery = 96% Analysis Date = 06/02/16 Pct Recovery = 96% Analysis Date = 05/28/16 Pct Recovery = 96% Analysis Date = 05/28/16 Pct Recovery = 96% Analysis Date = 05/23/16 Pct Recovery = 96% Analysis Date = 05/23/16 Pct Recovery = 96% Analysis Date = 05/18/16 Pct Recovery = 96% Analysis Date = 05/18/16 Pct Recovery = 96% Analysis Date = 05/13/16 Pct Recovery = 96% Analysis Date = 05/13/16 Pct Recovery = 96% Analysis Date = 05/09/16 Pct Recovery = 96% Analysis Date = 05/09/16 Pct Recovery = 96% Analysis Date = 05/04/16 Pct Recovery = 96% Analysis Date = 05/04/16 Pct Recovery = 96% Analysis Date = 04/29/16 Pct Recovery = 96% Analysis Date = 04/29/16 Pct Recovery = 96% Analysis Date = 04/24/16 Pct Recovery = 96% Analysis Date = 04/24/16 Pct Recovery = 96% Analysis Date = 04/19/16 Pct Recovery = 96% Analysis Date = 04/19/16 Pct Recovery = 96% Analysis Date = 04/15/16 Pct Recovery = 96% Analysis Date = 04/15/16 Pct Recovery = 96% Analysis Date = 04/10/16 Pct Recovery = 96% Analysis Date = 04/10/16 Pct Recovery = 96% Analysis Date = 04/05/16 Pct Recovery = 96% Analysis Date = 04/05/16 Pct Recovery = 96% Analysis Date = 03/31/16 Pct Recovery = 97% Analysis Date = 03/31/16 Pct Recovery = 97% Analysis Date = 03/26/16 Pct Recovery = 97% Analysis Date = 03/26/16 Pct Recovery = 97% Analysis Date = 03/22/16 Pct Recovery = 97% Analysis Date = 03/22/16 Pct Recovery = 97% Analysis Date = 03/17/16 Pct Recovery = 97% Analysis Date = 03/17/16 Pct Recovery = 97% Analysis Date = 03/12/16 Pct Recovery = 97% Analysis Date = 03/12/16 Pct Recovery = 97% Analysis Date = 03/07/16 Pct Recovery = 97% Analysis Date = 03/07/16 Pct Recovery = 97% Analysis Date = 03/02/16 Pct Recovery = 97% Analysis Date = 03/02/16 Pct Recovery = 97% Analysis Date = 02/27/16 Pct Recovery = 97% Analysis Date = 02/27/16 Pct Recovery = 97% Analysis Date = 02/22/16 Pct Recovery = 97% Analysis Date = 02/22/16 Pct Recovery = 97% Analysis Date = 02/17/16 Pct Recovery = 97% Analysis Date = 02/17/16 Pct Recovery = 97% Analysis Date = 02/12/16 Pct Recovery = 98% Analysis Date = 02/12/16 Pct Recovery = 98% Analysis Date = 02/07/16 Pct Recovery = 98% Analysis Date = 02/07/16 Pct Recovery = 98% Analysis Date = 02/03/16 Pct Recovery = 98% Analysis Date = 02/03/16 Pct Recovery = 98% Analysis Date = 01/29/16 Pct Recovery = 98% Analysis Date = 01/29/16 Pct Recovery = 98% Analysis Date = 01/24/16 Pct Recovery = 98% Analysis Date = 01/24/16 Pct Recovery = 98% Analysis Date = 01/19/16 Pct Recovery = 98% Analysis Date = 01/19/16 Pct Recovery = 98% Analysis Date = 01/14/16 Pct Recovery = 98% Analysis Date = 01/14/16 Pct Recovery = 98% Analysis Date = 01/10/16 Pct Recovery = 98% Analysis Date = 01/10/16 Pct Recovery = 98% Analysis Date = 01/05/16 Pct Recovery = 99% Analysis Date = 01/05/16 Pct Recovery = 99% Analysis Date = 12/31/15 Pct Recovery = 99% Analysis Date = 12/31/15 Pct Recovery = 99% Analysis Date = 12/26/15 Pct Recovery = 99% Analysis Date = 12/26/15 Pct Recovery = 99% Analysis Date = 12/21/15 Pct Recovery = 99% Analysis Date = 12/21/15 Pct Recovery = 99% Analysis Date = 12/17/15 Pct Recovery = 99% Analysis Date = 12/17/15 Pct Recovery = 99% Analysis Date = 12/12/15 Pct Recovery = 99% Analysis Date = 12/12/15 Pct Recovery = 99% Analysis Date = 12/07/15 Pct Recovery = 99% Analysis Date = 12/07/15 Pct Recovery = 99% Analysis Date = 12/02/15 Pct Recovery = 100% Analysis Date = 12/02/15 Pct Recovery = 100% Analysis Date = 11/27/15 Pct Recovery = 100% Analysis Date = 11/27/15 Pct Recovery = 100% Analysis Date = 11/23/15 Pct Recovery = 100% Analysis Date = 11/23/15 Pct Recovery = 100% Analysis Date = 11/18/15 Pct Recovery = 100% Analysis Date = 11/18/15 Pct Recovery = 100% Analysis Date = 11/13/15 Pct Recovery = 100% Analysis Date = 11/13/15 Pct Recovery = 100% Analysis Date = 11/08/15 Pct Recovery = 101% Analysis Date = 11/08/15 Pct Recovery = 101% Analysis Date = 11/03/15 Pct Recovery = 101% Analysis Date = 11/03/15 Pct Recovery = 101% Analysis Date = 10/30/15 Pct Recovery = 101% Analysis Date = 10/30/15 Pct Recovery = 101% Analysis Date = 10/25/15 Pct Recovery = 101% Analysis Date = 10/25/15 Pct Recovery = 101% Analysis Date = 10/20/15 Pct Recovery = 101% Analysis Date = 10/20/15 Pct Recovery = 101% Analysis Date = 10/15/15 Pct Recovery = 101% Analysis Date = 10/15/15 Pct Recovery = 101% Analysis Date = 10/10/15 Pct Recovery = 102% Analysis Date = 10/10/15 Pct Recovery = 102% Analysis Date = 10/06/15 Pct Recovery = 102% Analysis Date = 10/06/15 Pct Recovery = 102% Analysis Date = 10/01/15 Pct Recovery = 102% Analysis Date = 10/01/15 Pct Recovery = 102% Analysis Date = 09/26/15 Pct Recovery = 102% Analysis Date = 09/26/15 Pct Recovery = 102% Analysis Date = 09/21/15 Pct Recovery = 102% Analysis Date = 09/21/15 Pct Recovery = 102% Analysis Date = 09/16/15 Pct Recovery = 103% Analysis Date = 09/16/15 Pct Recovery = 103% Analysis Date = 09/12/15 Pct Recovery = 103% Analysis Date = 09/12/15 Pct Recovery = 103% Analysis Date = 09/07/15 Pct Recovery = 103% Analysis Date = 09/07/15 Pct Recovery = 103% Analysis Date = 09/02/15 Pct Recovery = 103% Analysis Date = 09/02/15 Pct Recovery = 103% Analysis Date = 08/28/15 Pct Recovery = 103% Analysis Date = 08/28/15 Pct Recovery = 103% Analysis Date = 08/23/15 Pct Recovery = 103% Analysis Date = 08/23/15 Pct Recovery = 103% Analysis Date = 08/19/15 Pct Recovery = 104% Analysis Date = 08/19/15 Pct Recovery = 104% Analysis Date = 08/14/15 Pct Recovery = 104% Analysis Date = 08/14/15 Pct Recovery = 104% Analysis Date = 08/09/15 Pct Recovery = 104% Analysis Date = 08/09/15 Pct Recovery = 104% Analysis Date = 08/04/15 Pct Recovery = 104% Analysis Date = 08/04/15 Pct Recovery = 104% Analysis Date = 07/30/15 Pct Recovery = 104% Analysis Date = 07/30/15 Pct Recovery = 104% Analysis Date = 07/26/15 Pct Recovery = 105% Analysis Date = 07/26/15 Pct Recovery = 105% Analysis Date = 07/21/15 Pct Recovery = 105% Analysis Date = 07/21/15 Pct Recovery = 105% Analysis Date = 07/16/15 Pct Recovery = 105% Analysis Date = 07/16/15 Pct Recovery = 105% Analysis Date = 07/11/15 Pct Recovery = 105% Analysis Date = 07/11/15 Pct Recovery = 105% Analysis Date = 07/06/15 Pct Recovery = 105% Analysis Date = 07/06/15 Pct Recovery = 105% Analysis Date = 07/02/15 Pct Recovery = 105% Analysis Date = 07/02/15 Pct Recovery = 105% Analysis Date = 06/27/15 Pct Recovery = 106% Analysis Date = 06/27/15 Pct Recovery = 106% Analysis Date = 06/22/15 Pct Recovery = 106% Analysis Date = 06/22/15 Pct Recovery = 106% Analysis Date = 06/17/15 Pct Recovery = 106% Analysis Date = 06/17/15 Pct Recovery = 106% Analysis Date = 06/12/15 Pct Recovery = 106% Analysis Date = 06/12/15 Pct Recovery = 106% Analysis Date = 06/08/15 Pct Recovery = 106% Analysis Date = 06/08/15 Pct Recovery = 106% Analysis Date = 06/03/15 Pct Recovery = 107% Analysis Date = 06/03/15 Pct Recovery = 107% Analysis Date = 05/29/15 Pct Recovery = 107% Analysis Date = 05/29/15 Pct Recovery = 107% Analysis Date = 05/24/15 Pct Recovery = 107% Analysis Date = 05/24/15 Pct Recovery = 107% Analysis Date = 05/19/15 Pct Recovery = 108% Analysis Date = 05/19/15 Pct Recovery = 108% Analysis Date = 05/15/15 Pct Recovery = 108% Analysis Date = 05/15/15 Pct Recovery = 108% Analysis Date = 05/10/15 Pct Recovery = 108% Analysis Date = 05/10/15 Pct Recovery = 108% Analysis Date = 05/05/15 Pct Recovery = 109% Analysis Date = 05/05/15 Pct Recovery = 109% Analysis Date = 04/30/15 Pct Recovery = 109% Analysis Date = 04/30/15 Pct Recovery = 109% Analysis Date = 04/25/15 Pct Recovery = 109% Analysis Date = 04/25/15 Pct Recovery = 109% Analysis Date = 04/21/15 Pct Recovery = 109% Analysis Date = 04/21/15 Pct Recovery = 109% Analysis Date = 04/16/15 Pct Recovery = 110% Analysis Date = 04/16/15 Pct Recovery = 110% Analysis Date = 04/11/15 Pct Recovery = 110% Analysis Date = 04/11/15 Pct Recovery = 110% Analysis Date = 04/06/15 Pct Recovery = 110% Analysis Date = 04/06/15 Pct Recovery = 110% Analysis Date = 04/01/15 Pct Recovery = 111% Analysis Date = 04/01/15 Pct Recovery = 111% Analysis Date = 03/28/15 Pct Recovery = 111% Analysis Date = 03/28/15 Pct Recovery = 111% Analysis Date = 03/23/15 Pct Recovery = 111% Analysis Date = 03/23/15 Pct Recovery = 111% Analysis Date = 03/18/15 Pct Recovery = 111% Analysis Date = 03/18/15 Pct Recovery = 111% Analysis Date = 03/13/15 Pct Recovery = 112% Analysis Date = 03/13/15 Pct Recovery = 112% Analysis Date = 03/08/15 Pct Recovery = 112% Analysis Date = 03/08/15 Pct Recovery = 112% Analysis Date = 03/04/15 Pct Recovery = 112% Analysis Date = 03/04/15 Pct Recovery = 112% Analysis Date = 02/27/15 Pct Recovery = 113% Analysis Date = 02/27/15 Pct Recovery = 113% Analysis Date = 02/22/15 Pct Recovery = 113% Analysis Date = 02/22/15 Pct Recovery = 113% Analysis Date = 02/17/15 Pct Recovery = 113% Analysis Date = 02/17/15 Pct Recovery = 113% Analysis Date = 02/12/15 Pct Recovery = 113% Analysis Date = 02/12/15 Pct Recovery = 113% Analysis Date = 02/08/15 Pct Recovery = 114% Analysis Date = 02/08/15 Pct Recovery = 114% Analysis Date = 02/03/15 Pct Recovery = 114% Analysis Date = 02/03/15 Pct Recovery = 114% Analysis Date = 01/29/15 Pct Recovery = 114% Analysis Date = 01/29/15 Pct Recovery = 114% Analysis Date = 01/24/15 Pct Recovery = 115% Analysis Date = 01/24/15 Pct Recovery = 115% Analysis Date = 01/19/15 Pct Recovery = 115% Analysis Date = 01/19/15 Pct Recovery = 115% Analysis Date = 01/15/15 Pct Recovery = 115% Analysis Date = 01/15/15 Pct Recovery = 115% Analysis Date = 01/10/15 Pct Recovery = 115% Analysis Date = 01/10/15 Pct Recovery = 115% Analysis Date = 01/05/15 Pct Recovery = 116% Analysis Date = 01/05/15 Pct Recovery = 116% Analysis Date = 12/31/14 Pct Recovery = 116% Analysis Date = 12/31/14 Pct Recovery = 116% Analysis Date = 12/26/14 Pct Recovery = 116% Analysis Date = 12/26/14 Pct Recovery = 116% Analysis Date = 12/22/14 Pct Recovery = 117% Analysis Date = 12/22/14 Pct Recovery = 117% Analysis Date = 12/17/14 Pct Recovery = 117% Analysis Date = 12/17/14 Pct Recovery = 117% Analysis Date = 12/12/14 Pct Recovery = 117% Analysis Date = 12/12/14 Pct Recovery = 117% Analysis Date = 12/07/14 Pct Recovery = 117% Analysis Date = 12/07/14 Pct Recovery = 117% Analysis Date = 12/02/14 Pct Recovery = 118% Analysis Date = 12/02/14 Pct Recovery = 118% Analysis Date = 11/28/14 Pct Recovery = 118% Analysis Date = 11/28/14 Pct Recovery = 118% Analysis Date = 11/23/14 Pct Recovery = 118% Analysis Date = 11/23/14 Pct Recovery = 118% Analysis Date = 11/18/14 Pct Recovery = 119% Analysis Date = 11/18/14 Pct Recovery = 119% Analysis Date = 11/13/14 Pct Recovery = 119% Analysis Date = 11/13/14 Pct Recovery = 119% Analysis Date = 11/08/14 Pct Recovery = 119% Analysis Date = 11/08/14 Pct Recovery = 119% Analysis Date = 11/04/14 Pct Recovery = 120% Analysis Date = 11/04/14 Pct Recovery = 120% Analysis Date = 10/30/14 Pct Recovery = 120% Analysis Date = 10/30/14 Pct Recovery = 120% Analysis Date = 10/25/14 Pct Recovery = 120% Analysis Date = 10/25/14 Pct Recovery = 120% Analysis Date = 10/20/14 Pct Recovery = 121% Analysis Date = 10/20/14 Pct Recovery = 121% Analysis Date = 10/15/14 Pct Recovery = 121% Analysis Date = 10/15/14 Pct Recovery = 121% Analysis Date = 10/11/14 Pct Recovery = 121% Analysis Date = 10/11/14 Pct Recovery = 121% Analysis Date = 10/06/14 Pct Recovery = 121% Analysis Date = 10/06/14 Pct Recovery = 121% Analysis Date = 10/01/14 Pct Recovery = 122% Analysis Date = 10/01/14 Pct Recovery = 122% Analysis Date = 09/26/14 Pct Recovery = 122% Analysis Date = 09/26/14 Pct Recovery = 122% Analysis Date = 09/21/14 Pct Recovery = 122% Analysis Date = 09/21/14 Pct Recovery = 122% Analysis Date = 09/17/14 Pct Recovery = 123% Analysis Date = 09/17/14 Pct Recovery = 123% Analysis Date = 09/12/14 Pct Recovery = 123% Analysis Date = 09/12/14 Pct Recovery = 123% Analysis Date = 09/07/14 Pct Recovery = 123% Analysis Date = 09/07/14 Pct Recovery = 123% Analysis Date = 09/02/14 Pct Recovery = 124% Analysis Date = 09/02/14 Pct Recovery = 124% Analysis Date = 08/28/14 Pct Recovery = 124% Analysis Date = 08/28/14 Pct Recovery = 124% Analysis Date = 08/24/14 Pct Recovery = 124% Analysis Date = 08/24/14 Pct Recovery = 124% Analysis Date = 08/19/14 Pct Recovery = 125% Analysis Date = 08/19/14 Pct Recovery = 125% Analysis Date = 08/14/14 Pct Recovery = 125% Analysis Date = 08/14/14 Pct Recovery = 125% Analysis Date = 08/09/14 Pct Recovery = 125% Analysis Date = 08/09/14 Pct Recovery = 125% Analysis Date = 08/04/14 Pct Recovery = 126% Analysis Date = 08/04/14 Pct Recovery = 126% Analysis Date = 07/31/14 Pct Recovery = 126% Analysis Date = 07/31/14 Pct Recovery = 126% Analysis Date = 07/26/14 Pct Recovery = 126% Analysis Date = 07/26/14 Pct Recovery = 126% Analysis Date = 07/21/14 Pct Recovery = 127% Analysis Date = 07/21/14 Pct Recovery = 127% Analysis Date = 07/16/14 Pct Recovery = 127% Analysis Date = 07/16/14 Pct Recovery = 127% Analysis Date = 07/11/14 Pct Recovery = 127% Analysis Date = 07/11/14 Pct Recovery = 127% Analysis Date = 07/07/14 Pct Recovery = 128% Analysis Date = 07/07/14 Pct Recovery = 128% Analysis Date = 07/02/14 Pct Recovery = 128% Analysis Date = 07/02/14 Pct Recovery = 128% Analysis Date = 06/27/14 Pct Recovery = 128% Analysis Date = 06/27/14 Pct Recovery = 128% Analysis Date = 06/22/14 Pct Recovery = 129% Analysis Date = 06/22/14 Pct Recovery = 129% Analysis Date = 06/17/14 Pct Recovery = 129% Analysis Date = 06/17/14 Pct Recovery = 129% Analysis Date = 06/13/14 Pct Recovery = 129% Analysis Date = 06/13/14 Pct Recovery = 129% Analysis Date = 06/08/14 Pct Recovery = 130% Analysis Date = 06/08/14 Pct Recovery = 130% Analysis Date = 06/03/14 Pct Recovery = 130% Analysis Date = 06/03/14 Pct Recovery = 130% Analysis Date = 05/29/14 Pct Recovery = 130% Analysis Date = 05/29/14 Pct Recovery = 130% Analysis Date = 05/24/14 Pct Recovery = 131% Analysis Date = 05/24/14 Pct Recovery = 131% Analysis Date = 05/20/14 Pct Recovery = 131% Analysis Date = 05/20/14 Pct Recovery = 131% Analysis Date = 05/15/14 Pct Recovery = 131% Analysis Date = 05/15/14 Pct Recovery = 131% Analysis Date = 05/10/14 Pct Recovery = 132% Analysis Date = 05/10/14 Pct Recovery = 132% Analysis Date = 05/05/14 Pct Recovery = 132% Analysis Date = 05/05/14 Pct Recovery = 132% Analysis Date = 05/01/14 Pct Recovery = 132% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
1,1,2-TRICHLOROTRIFLUOROETHANE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 50 106% 20% 99% 19%
Total 50 106% 20% 99% 19%

Sample Statistics
1,1,2-TRICHLOROTRIFLUOROETHANE

Characteristic N % % Basis
Plotted 50 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 50 .  
False Negatives 0 0% 0 out of 50
Not Spiked 23 .  
False Positives 0 0% 0 out of 23

BQS OBSP Determination:
1,1-DICHLOROETHANE
METHOD: 4440 , TESTIDCODE: 34496GCM66
Open Data Set

Analysis Date = 12/16/16 SpikeMix = NSI 041816AVOC: 40 µl & ChemService 5082900: 40 µl Pct Recovery = 100% Analysis Date = 07/14/16 SpikeMix = Accu 216041125: 40 µl & NSI 041816AVOC: 40 µl Pct Recovery = 109% Analysis Date = 12/12/16 SpikeMix = Accu 216041125: 40 µl & Crescent 03FF058: 40 µl Pct Recovery = 101% Analysis Date = 08/04/16 SpikeMix = Crescent 03FF058: 40 µl & Supelco LC20141V: 40 µl Pct Recovery = 99% Analysis Date = 08/26/16 SpikeMix = NSI 041816AVOC: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 99% Analysis Date = 11/21/16 SpikeMix = Crescent 03FF058: 25 µl & Supelco LC20141V: 25 µl Pct Recovery = 94% Analysis Date = 06/30/16 SpikeMix = Crescent 03FF058: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 97% Analysis Date = 06/21/16 SpikeMix = Phenova B20160319: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 94% Analysis Date = 05/24/16 SpikeMix = Accu 216041125: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 92% Analysis Date = 03/19/15 SpikeMix = Spex Organics C1140417015: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 121% Analysis Date = 03/06/15 SpikeMix = ERA 0227-14-06.1A: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 91% Analysis Date = 12/17/14 SpikeMix = Supelco LC06438: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 92% Analysis Date = 11/22/14 SpikeMix = NSI 032614: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 103% Analysis Date = 09/21/14 SpikeMix = Supelco LC06438: 20 µl Pct Recovery = 97% Analysis Date = 08/19/14 SpikeMix = Spex Organics C1140417015: 20 µl & Accu 214031115: 20 µl Pct Recovery = 116% Analysis Date = 08/16/14 SpikeMix = ERA 0227-14-06.1A: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 115% Analysis Date = 06/10/14 SpikeMix = NSI 032614: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 96% Analysis Date = 09/29/15 SpikeMix = Accu 215041380: 25 µl & ERA 0406-15-03: 25 µl Pct Recovery = 88% Analysis Date = 08/15/15 SpikeMix = Supelco LC13545: 25 µl & Crescent 04EE008: 25 µl Pct Recovery = 99% Analysis Date = 07/13/15 SpikeMix = Crescent 04EE008: 25 µl & NSI 050515AVOC: 25 µl Pct Recovery = 98% Analysis Date = 10/13/16 SpikeMix = Accu 216041125: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 105% Analysis Date = 10/13/16 SpikeMix = NSI 041816AVOC: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 95% Analysis Date = 07/29/16 SpikeMix = Phenova B20160319: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 101% Analysis Date = 06/10/16 SpikeMix = NSI 041816AVOC: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 114% Analysis Date = 09/28/16 SpikeMix = Crescent 03FF058: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 99% Analysis Date = 09/08/16 SpikeMix = Phenova B20160319: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 95% Analysis Date = 08/20/16 SpikeMix = Accu 216041125: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 100% Analysis Date = 04/02/16 SpikeMix = Supelco LC13545: 15 µl & Accu 215041380: 15 µl Pct Recovery = 89% Analysis Date = 03/04/16 SpikeMix = Accu 215041380: 15 µl & ERA 0406-15-03: 15 µl Pct Recovery = 86% Analysis Date = 06/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Accu 215041380: 15 µl Pct Recovery = 86% Analysis Date = 12/18/15 SpikeMix = Supelco LC13545: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 86% Analysis Date = 10/17/15 SpikeMix = Crescent 04EE008: 15 µl & NSI 050515AVOC: 15 µl Pct Recovery = 88% Analysis Date = 05/09/15 SpikeMix = Spex Organics EN150428007: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 98% Analysis Date = 11/06/14 SpikeMix = Spex Organics C1140417015: 10 µl & Crescent 03DD004: 10 µl Pct Recovery = 107% Analysis Date = 10/21/14 SpikeMix = ERA 0227-14-06.1A: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 88% Analysis Date = 09/09/14 SpikeMix = NSI 032614: 10 µl & Spex Organics C1140417015: 10 µl Pct Recovery = 112% Analysis Date = 07/23/14 SpikeMix = Spex Organics C1140417015: 10 µl & Accu 214031115: 10 µl Pct Recovery = 127% Analysis Date = 07/11/14 SpikeMix = Spex Organics C1140417015: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 112% Analysis Date = 06/18/14 SpikeMix = Supelco LC06438: 10 µl & Accu 214031115: 10 µl Pct Recovery = 105% Analysis Date = 05/30/14 SpikeMix = NSI 032614: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 84% Analysis Date = 05/03/14 SpikeMix = Crescent 03DD004: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 98% Analysis Date = 02/18/16 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 89% Analysis Date = 11/20/15 SpikeMix = Accu 215041380: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 88% Analysis Date = 11/12/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 94% Analysis Date = 05/21/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 94% Analysis Date = 05/13/16 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 93% Analysis Date = 01/27/16 SpikeMix = Crescent 04EE008: 10 µl & NSI 050515AVOC: 10 µl Pct Recovery = 111% Analysis Date = 07/31/15 SpikeMix = Crescent 04EE008: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 86% Analysis Date = 05/09/15 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 102% Analysis Date = 12/16/16 Pct Recovery = 101% Analysis Date = 12/11/16 Pct Recovery = 101% Analysis Date = 12/11/16 Pct Recovery = 101% Analysis Date = 12/06/16 Pct Recovery = 101% Analysis Date = 12/06/16 Pct Recovery = 101% Analysis Date = 12/01/16 Pct Recovery = 101% Analysis Date = 12/01/16 Pct Recovery = 101% Analysis Date = 11/26/16 Pct Recovery = 101% Analysis Date = 11/26/16 Pct Recovery = 101% Analysis Date = 11/22/16 Pct Recovery = 101% Analysis Date = 11/22/16 Pct Recovery = 101% Analysis Date = 11/17/16 Pct Recovery = 101% Analysis Date = 11/17/16 Pct Recovery = 101% Analysis Date = 11/12/16 Pct Recovery = 101% Analysis Date = 11/12/16 Pct Recovery = 101% Analysis Date = 11/07/16 Pct Recovery = 100% Analysis Date = 11/07/16 Pct Recovery = 100% Analysis Date = 11/02/16 Pct Recovery = 100% Analysis Date = 11/02/16 Pct Recovery = 100% Analysis Date = 10/29/16 Pct Recovery = 100% Analysis Date = 10/29/16 Pct Recovery = 100% Analysis Date = 10/24/16 Pct Recovery = 100% Analysis Date = 10/24/16 Pct Recovery = 100% Analysis Date = 10/19/16 Pct Recovery = 100% Analysis Date = 10/19/16 Pct Recovery = 100% Analysis Date = 10/14/16 Pct Recovery = 100% Analysis Date = 10/14/16 Pct Recovery = 100% Analysis Date = 10/09/16 Pct Recovery = 100% Analysis Date = 10/09/16 Pct Recovery = 100% Analysis Date = 10/05/16 Pct Recovery = 100% Analysis Date = 10/05/16 Pct Recovery = 100% Analysis Date = 09/30/16 Pct Recovery = 100% Analysis Date = 09/30/16 Pct Recovery = 100% Analysis Date = 09/25/16 Pct Recovery = 99% Analysis Date = 09/25/16 Pct Recovery = 99% Analysis Date = 09/20/16 Pct Recovery = 99% Analysis Date = 09/20/16 Pct Recovery = 99% Analysis Date = 09/15/16 Pct Recovery = 99% Analysis Date = 09/15/16 Pct Recovery = 99% Analysis Date = 09/11/16 Pct Recovery = 99% Analysis Date = 09/11/16 Pct Recovery = 99% Analysis Date = 09/06/16 Pct Recovery = 99% Analysis Date = 09/06/16 Pct Recovery = 99% Analysis Date = 09/01/16 Pct Recovery = 99% Analysis Date = 09/01/16 Pct Recovery = 99% Analysis Date = 08/27/16 Pct Recovery = 99% Analysis Date = 08/27/16 Pct Recovery = 99% Analysis Date = 08/23/16 Pct Recovery = 99% Analysis Date = 08/23/16 Pct Recovery = 99% Analysis Date = 08/18/16 Pct Recovery = 99% Analysis Date = 08/18/16 Pct Recovery = 99% Analysis Date = 08/13/16 Pct Recovery = 98% Analysis Date = 08/13/16 Pct Recovery = 98% Analysis Date = 08/08/16 Pct Recovery = 98% Analysis Date = 08/08/16 Pct Recovery = 98% Analysis Date = 08/03/16 Pct Recovery = 98% Analysis Date = 08/03/16 Pct Recovery = 98% Analysis Date = 07/30/16 Pct Recovery = 98% Analysis Date = 07/30/16 Pct Recovery = 98% Analysis Date = 07/25/16 Pct Recovery = 98% Analysis Date = 07/25/16 Pct Recovery = 98% Analysis Date = 07/20/16 Pct Recovery = 98% Analysis Date = 07/20/16 Pct Recovery = 98% Analysis Date = 07/15/16 Pct Recovery = 98% Analysis Date = 07/15/16 Pct Recovery = 98% Analysis Date = 07/10/16 Pct Recovery = 98% Analysis Date = 07/10/16 Pct Recovery = 98% Analysis Date = 07/06/16 Pct Recovery = 98% Analysis Date = 07/06/16 Pct Recovery = 98% Analysis Date = 07/01/16 Pct Recovery = 97% Analysis Date = 07/01/16 Pct Recovery = 97% Analysis Date = 06/26/16 Pct Recovery = 97% Analysis Date = 06/26/16 Pct Recovery = 97% Analysis Date = 06/21/16 Pct Recovery = 97% Analysis Date = 06/21/16 Pct Recovery = 97% Analysis Date = 06/16/16 Pct Recovery = 97% Analysis Date = 06/16/16 Pct Recovery = 97% Analysis Date = 06/12/16 Pct Recovery = 97% Analysis Date = 06/12/16 Pct Recovery = 97% Analysis Date = 06/07/16 Pct Recovery = 97% Analysis Date = 06/07/16 Pct Recovery = 97% Analysis Date = 06/02/16 Pct Recovery = 97% Analysis Date = 06/02/16 Pct Recovery = 97% Analysis Date = 05/28/16 Pct Recovery = 97% Analysis Date = 05/28/16 Pct Recovery = 97% Analysis Date = 05/24/16 Pct Recovery = 97% Analysis Date = 05/24/16 Pct Recovery = 97% Analysis Date = 05/19/16 Pct Recovery = 96% Analysis Date = 05/19/16 Pct Recovery = 96% Analysis Date = 05/14/16 Pct Recovery = 96% Analysis Date = 05/14/16 Pct Recovery = 96% Analysis Date = 05/09/16 Pct Recovery = 96% Analysis Date = 05/09/16 Pct Recovery = 96% Analysis Date = 05/04/16 Pct Recovery = 96% Analysis Date = 05/04/16 Pct Recovery = 96% Analysis Date = 04/30/16 Pct Recovery = 96% Analysis Date = 04/30/16 Pct Recovery = 96% Analysis Date = 04/25/16 Pct Recovery = 96% Analysis Date = 04/25/16 Pct Recovery = 96% Analysis Date = 04/20/16 Pct Recovery = 96% Analysis Date = 04/20/16 Pct Recovery = 96% Analysis Date = 04/15/16 Pct Recovery = 96% Analysis Date = 04/15/16 Pct Recovery = 96% Analysis Date = 04/10/16 Pct Recovery = 95% Analysis Date = 04/10/16 Pct Recovery = 95% Analysis Date = 04/06/16 Pct Recovery = 95% Analysis Date = 04/06/16 Pct Recovery = 95% Analysis Date = 04/01/16 Pct Recovery = 95% Analysis Date = 04/01/16 Pct Recovery = 95% Analysis Date = 03/27/16 Pct Recovery = 95% Analysis Date = 03/27/16 Pct Recovery = 95% Analysis Date = 03/22/16 Pct Recovery = 95% Analysis Date = 03/22/16 Pct Recovery = 95% Analysis Date = 03/17/16 Pct Recovery = 95% Analysis Date = 03/17/16 Pct Recovery = 95% Analysis Date = 03/13/16 Pct Recovery = 95% Analysis Date = 03/13/16 Pct Recovery = 95% Analysis Date = 03/08/16 Pct Recovery = 95% Analysis Date = 03/08/16 Pct Recovery = 95% Analysis Date = 03/03/16 Pct Recovery = 94% Analysis Date = 03/03/16 Pct Recovery = 94% Analysis Date = 02/27/16 Pct Recovery = 94% Analysis Date = 02/27/16 Pct Recovery = 94% Analysis Date = 02/23/16 Pct Recovery = 94% Analysis Date = 02/23/16 Pct Recovery = 94% Analysis Date = 02/18/16 Pct Recovery = 94% Analysis Date = 02/18/16 Pct Recovery = 94% Analysis Date = 02/13/16 Pct Recovery = 94% Analysis Date = 02/13/16 Pct Recovery = 94% Analysis Date = 02/08/16 Pct Recovery = 94% Analysis Date = 02/08/16 Pct Recovery = 94% Analysis Date = 02/03/16 Pct Recovery = 94% Analysis Date = 02/03/16 Pct Recovery = 94% Analysis Date = 01/30/16 Pct Recovery = 94% Analysis Date = 01/30/16 Pct Recovery = 94% Analysis Date = 01/25/16 Pct Recovery = 94% Analysis Date = 01/25/16 Pct Recovery = 94% Analysis Date = 01/20/16 Pct Recovery = 94% Analysis Date = 01/20/16 Pct Recovery = 94% Analysis Date = 01/15/16 Pct Recovery = 94% Analysis Date = 01/15/16 Pct Recovery = 94% Analysis Date = 01/10/16 Pct Recovery = 93% Analysis Date = 01/10/16 Pct Recovery = 93% Analysis Date = 01/06/16 Pct Recovery = 93% Analysis Date = 01/06/16 Pct Recovery = 93% Analysis Date = 01/01/16 Pct Recovery = 93% Analysis Date = 01/01/16 Pct Recovery = 93% Analysis Date = 12/27/15 Pct Recovery = 93% Analysis Date = 12/27/15 Pct Recovery = 93% Analysis Date = 12/22/15 Pct Recovery = 93% Analysis Date = 12/22/15 Pct Recovery = 93% Analysis Date = 12/17/15 Pct Recovery = 93% Analysis Date = 12/17/15 Pct Recovery = 93% Analysis Date = 12/13/15 Pct Recovery = 93% Analysis Date = 12/13/15 Pct Recovery = 93% Analysis Date = 12/08/15 Pct Recovery = 93% Analysis Date = 12/08/15 Pct Recovery = 93% Analysis Date = 12/03/15 Pct Recovery = 93% Analysis Date = 12/03/15 Pct Recovery = 93% Analysis Date = 11/28/15 Pct Recovery = 93% Analysis Date = 11/28/15 Pct Recovery = 93% Analysis Date = 11/24/15 Pct Recovery = 93% Analysis Date = 11/24/15 Pct Recovery = 93% Analysis Date = 11/19/15 Pct Recovery = 93% Analysis Date = 11/19/15 Pct Recovery = 93% Analysis Date = 11/14/15 Pct Recovery = 93% Analysis Date = 11/14/15 Pct Recovery = 93% Analysis Date = 11/09/15 Pct Recovery = 93% Analysis Date = 11/09/15 Pct Recovery = 93% Analysis Date = 11/04/15 Pct Recovery = 93% Analysis Date = 11/04/15 Pct Recovery = 93% Analysis Date = 10/31/15 Pct Recovery = 93% Analysis Date = 10/31/15 Pct Recovery = 93% Analysis Date = 10/26/15 Pct Recovery = 93% Analysis Date = 10/26/15 Pct Recovery = 93% Analysis Date = 10/21/15 Pct Recovery = 93% Analysis Date = 10/21/15 Pct Recovery = 93% Analysis Date = 10/16/15 Pct Recovery = 93% Analysis Date = 10/16/15 Pct Recovery = 93% Analysis Date = 10/11/15 Pct Recovery = 93% Analysis Date = 10/11/15 Pct Recovery = 93% Analysis Date = 10/07/15 Pct Recovery = 93% Analysis Date = 10/07/15 Pct Recovery = 93% Analysis Date = 10/02/15 Pct Recovery = 94% Analysis Date = 10/02/15 Pct Recovery = 94% Analysis Date = 09/27/15 Pct Recovery = 94% Analysis Date = 09/27/15 Pct Recovery = 94% Analysis Date = 09/22/15 Pct Recovery = 94% Analysis Date = 09/22/15 Pct Recovery = 94% Analysis Date = 09/17/15 Pct Recovery = 94% Analysis Date = 09/17/15 Pct Recovery = 94% Analysis Date = 09/13/15 Pct Recovery = 94% Analysis Date = 09/13/15 Pct Recovery = 94% Analysis Date = 09/08/15 Pct Recovery = 94% Analysis Date = 09/08/15 Pct Recovery = 94% Analysis Date = 09/03/15 Pct Recovery = 94% Analysis Date = 09/03/15 Pct Recovery = 94% Analysis Date = 08/29/15 Pct Recovery = 94% Analysis Date = 08/29/15 Pct Recovery = 94% Analysis Date = 08/25/15 Pct Recovery = 94% Analysis Date = 08/25/15 Pct Recovery = 94% Analysis Date = 08/20/15 Pct Recovery = 94% Analysis Date = 08/20/15 Pct Recovery = 94% Analysis Date = 08/15/15 Pct Recovery = 94% Analysis Date = 08/15/15 Pct Recovery = 94% Analysis Date = 08/10/15 Pct Recovery = 94% Analysis Date = 08/10/15 Pct Recovery = 94% Analysis Date = 08/05/15 Pct Recovery = 95% Analysis Date = 08/05/15 Pct Recovery = 95% Analysis Date = 08/01/15 Pct Recovery = 95% Analysis Date = 08/01/15 Pct Recovery = 95% Analysis Date = 07/27/15 Pct Recovery = 95% Analysis Date = 07/27/15 Pct Recovery = 95% Analysis Date = 07/22/15 Pct Recovery = 95% Analysis Date = 07/22/15 Pct Recovery = 95% Analysis Date = 07/17/15 Pct Recovery = 95% Analysis Date = 07/17/15 Pct Recovery = 95% Analysis Date = 07/12/15 Pct Recovery = 95% Analysis Date = 07/12/15 Pct Recovery = 95% Analysis Date = 07/08/15 Pct Recovery = 95% Analysis Date = 07/08/15 Pct Recovery = 95% Analysis Date = 07/03/15 Pct Recovery = 95% Analysis Date = 07/03/15 Pct Recovery = 95% Analysis Date = 06/28/15 Pct Recovery = 95% Analysis Date = 06/28/15 Pct Recovery = 95% Analysis Date = 06/23/15 Pct Recovery = 95% Analysis Date = 06/23/15 Pct Recovery = 95% Analysis Date = 06/18/15 Pct Recovery = 96% Analysis Date = 06/18/15 Pct Recovery = 96% Analysis Date = 06/14/15 Pct Recovery = 96% Analysis Date = 06/14/15 Pct Recovery = 96% Analysis Date = 06/09/15 Pct Recovery = 96% Analysis Date = 06/09/15 Pct Recovery = 96% Analysis Date = 06/04/15 Pct Recovery = 96% Analysis Date = 06/04/15 Pct Recovery = 96% Analysis Date = 05/30/15 Pct Recovery = 96% Analysis Date = 05/30/15 Pct Recovery = 96% Analysis Date = 05/25/15 Pct Recovery = 96% Analysis Date = 05/25/15 Pct Recovery = 96% Analysis Date = 05/21/15 Pct Recovery = 96% Analysis Date = 05/21/15 Pct Recovery = 96% Analysis Date = 05/16/15 Pct Recovery = 96% Analysis Date = 05/16/15 Pct Recovery = 96% Analysis Date = 05/11/15 Pct Recovery = 97% Analysis Date = 05/11/15 Pct Recovery = 97% Analysis Date = 05/06/15 Pct Recovery = 97% Analysis Date = 05/06/15 Pct Recovery = 97% Analysis Date = 05/02/15 Pct Recovery = 97% Analysis Date = 05/02/15 Pct Recovery = 97% Analysis Date = 04/27/15 Pct Recovery = 97% Analysis Date = 04/27/15 Pct Recovery = 97% Analysis Date = 04/22/15 Pct Recovery = 97% Analysis Date = 04/22/15 Pct Recovery = 97% Analysis Date = 04/17/15 Pct Recovery = 97% Analysis Date = 04/17/15 Pct Recovery = 97% Analysis Date = 04/12/15 Pct Recovery = 98% Analysis Date = 04/12/15 Pct Recovery = 98% Analysis Date = 04/08/15 Pct Recovery = 98% Analysis Date = 04/08/15 Pct Recovery = 98% Analysis Date = 04/03/15 Pct Recovery = 98% Analysis Date = 04/03/15 Pct Recovery = 98% Analysis Date = 03/29/15 Pct Recovery = 98% Analysis Date = 03/29/15 Pct Recovery = 98% Analysis Date = 03/24/15 Pct Recovery = 98% Analysis Date = 03/24/15 Pct Recovery = 98% Analysis Date = 03/19/15 Pct Recovery = 98% Analysis Date = 03/19/15 Pct Recovery = 98% Analysis Date = 03/15/15 Pct Recovery = 99% Analysis Date = 03/15/15 Pct Recovery = 99% Analysis Date = 03/10/15 Pct Recovery = 99% Analysis Date = 03/10/15 Pct Recovery = 99% Analysis Date = 03/05/15 Pct Recovery = 99% Analysis Date = 03/05/15 Pct Recovery = 99% Analysis Date = 02/28/15 Pct Recovery = 99% Analysis Date = 02/28/15 Pct Recovery = 99% Analysis Date = 02/23/15 Pct Recovery = 99% Analysis Date = 02/23/15 Pct Recovery = 99% Analysis Date = 02/19/15 Pct Recovery = 99% Analysis Date = 02/19/15 Pct Recovery = 99% Analysis Date = 02/14/15 Pct Recovery = 99% Analysis Date = 02/14/15 Pct Recovery = 99% Analysis Date = 02/09/15 Pct Recovery = 100% Analysis Date = 02/09/15 Pct Recovery = 100% Analysis Date = 02/04/15 Pct Recovery = 100% Analysis Date = 02/04/15 Pct Recovery = 100% Analysis Date = 01/31/15 Pct Recovery = 100% Analysis Date = 01/31/15 Pct Recovery = 100% Analysis Date = 01/26/15 Pct Recovery = 100% Analysis Date = 01/26/15 Pct Recovery = 100% Analysis Date = 01/21/15 Pct Recovery = 100% Analysis Date = 01/21/15 Pct Recovery = 100% Analysis Date = 01/16/15 Pct Recovery = 100% Analysis Date = 01/16/15 Pct Recovery = 100% Analysis Date = 01/11/15 Pct Recovery = 100% Analysis Date = 01/11/15 Pct Recovery = 100% Analysis Date = 01/07/15 Pct Recovery = 101% Analysis Date = 01/07/15 Pct Recovery = 101% Analysis Date = 01/02/15 Pct Recovery = 101% Analysis Date = 01/02/15 Pct Recovery = 101% Analysis Date = 12/28/14 Pct Recovery = 101% Analysis Date = 12/28/14 Pct Recovery = 101% Analysis Date = 12/23/14 Pct Recovery = 101% Analysis Date = 12/23/14 Pct Recovery = 101% Analysis Date = 12/18/14 Pct Recovery = 101% Analysis Date = 12/18/14 Pct Recovery = 101% Analysis Date = 12/14/14 Pct Recovery = 101% Analysis Date = 12/14/14 Pct Recovery = 101% Analysis Date = 12/09/14 Pct Recovery = 101% Analysis Date = 12/09/14 Pct Recovery = 101% Analysis Date = 12/04/14 Pct Recovery = 101% Analysis Date = 12/04/14 Pct Recovery = 101% Analysis Date = 11/29/14 Pct Recovery = 102% Analysis Date = 11/29/14 Pct Recovery = 102% Analysis Date = 11/24/14 Pct Recovery = 102% Analysis Date = 11/24/14 Pct Recovery = 102% Analysis Date = 11/20/14 Pct Recovery = 102% Analysis Date = 11/20/14 Pct Recovery = 102% Analysis Date = 11/15/14 Pct Recovery = 102% Analysis Date = 11/15/14 Pct Recovery = 102% Analysis Date = 11/10/14 Pct Recovery = 102% Analysis Date = 11/10/14 Pct Recovery = 102% Analysis Date = 11/05/14 Pct Recovery = 102% Analysis Date = 11/05/14 Pct Recovery = 102% Analysis Date = 11/01/14 Pct Recovery = 102% Analysis Date = 11/01/14 Pct Recovery = 102% Analysis Date = 10/27/14 Pct Recovery = 102% Analysis Date = 10/27/14 Pct Recovery = 102% Analysis Date = 10/22/14 Pct Recovery = 102% Analysis Date = 10/22/14 Pct Recovery = 102% Analysis Date = 10/17/14 Pct Recovery = 103% Analysis Date = 10/17/14 Pct Recovery = 103% Analysis Date = 10/12/14 Pct Recovery = 103% Analysis Date = 10/12/14 Pct Recovery = 103% Analysis Date = 10/08/14 Pct Recovery = 103% Analysis Date = 10/08/14 Pct Recovery = 103% Analysis Date = 10/03/14 Pct Recovery = 103% Analysis Date = 10/03/14 Pct Recovery = 103% Analysis Date = 09/28/14 Pct Recovery = 103% Analysis Date = 09/28/14 Pct Recovery = 103% Analysis Date = 09/23/14 Pct Recovery = 103% Analysis Date = 09/23/14 Pct Recovery = 103% Analysis Date = 09/18/14 Pct Recovery = 103% Analysis Date = 09/18/14 Pct Recovery = 103% Analysis Date = 09/14/14 Pct Recovery = 103% Analysis Date = 09/14/14 Pct Recovery = 103% Analysis Date = 09/09/14 Pct Recovery = 103% Analysis Date = 09/09/14 Pct Recovery = 103% Analysis Date = 09/04/14 Pct Recovery = 103% Analysis Date = 09/04/14 Pct Recovery = 103% Analysis Date = 08/30/14 Pct Recovery = 104% Analysis Date = 08/30/14 Pct Recovery = 104% Analysis Date = 08/25/14 Pct Recovery = 104% Analysis Date = 08/25/14 Pct Recovery = 104% Analysis Date = 08/21/14 Pct Recovery = 104% Analysis Date = 08/21/14 Pct Recovery = 104% Analysis Date = 08/16/14 Pct Recovery = 104% Analysis Date = 08/16/14 Pct Recovery = 104% Analysis Date = 08/11/14 Pct Recovery = 104% Analysis Date = 08/11/14 Pct Recovery = 104% Analysis Date = 08/06/14 Pct Recovery = 104% Analysis Date = 08/06/14 Pct Recovery = 104% Analysis Date = 08/02/14 Pct Recovery = 104% Analysis Date = 08/02/14 Pct Recovery = 104% Analysis Date = 07/28/14 Pct Recovery = 104% Analysis Date = 07/28/14 Pct Recovery = 104% Analysis Date = 07/23/14 Pct Recovery = 104% Analysis Date = 07/23/14 Pct Recovery = 104% Analysis Date = 07/18/14 Pct Recovery = 105% Analysis Date = 07/18/14 Pct Recovery = 105% Analysis Date = 07/13/14 Pct Recovery = 105% Analysis Date = 07/13/14 Pct Recovery = 105% Analysis Date = 07/09/14 Pct Recovery = 105% Analysis Date = 07/09/14 Pct Recovery = 105% Analysis Date = 07/04/14 Pct Recovery = 105% Analysis Date = 07/04/14 Pct Recovery = 105% Analysis Date = 06/29/14 Pct Recovery = 105% Analysis Date = 06/29/14 Pct Recovery = 105% Analysis Date = 06/24/14 Pct Recovery = 105% Analysis Date = 06/24/14 Pct Recovery = 105% Analysis Date = 06/19/14 Pct Recovery = 105% Analysis Date = 06/19/14 Pct Recovery = 105% Analysis Date = 06/15/14 Pct Recovery = 105% Analysis Date = 06/15/14 Pct Recovery = 105% Analysis Date = 06/10/14 Pct Recovery = 105% Analysis Date = 06/10/14 Pct Recovery = 105% Analysis Date = 06/05/14 Pct Recovery = 105% Analysis Date = 06/05/14 Pct Recovery = 105% Analysis Date = 05/31/14 Pct Recovery = 105% Analysis Date = 05/31/14 Pct Recovery = 105% Analysis Date = 05/26/14 Pct Recovery = 106% Analysis Date = 05/26/14 Pct Recovery = 106% Analysis Date = 05/22/14 Pct Recovery = 106% Analysis Date = 05/22/14 Pct Recovery = 106% Analysis Date = 05/17/14 Pct Recovery = 106% Analysis Date = 05/17/14 Pct Recovery = 106% Analysis Date = 05/12/14 Pct Recovery = 106% Analysis Date = 05/12/14 Pct Recovery = 106% Analysis Date = 05/07/14 Pct Recovery = 106% Analysis Date = 05/07/14 Pct Recovery = 106% Analysis Date = 05/03/14 Pct Recovery = 106% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
1,1-DICHLOROETHANE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 49 99% 10% 98% 9%
Total 49 99% 10% 98% 9%

Sample Statistics
1,1-DICHLOROETHANE

Characteristic N % % Basis
Plotted 49 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 49 .  
False Negatives 0 0% 0 out of 49
Not Spiked 24 .  
False Positives 0 0% 0 out of 24

BQS OBSP Determination:
1,1-DICHLOROETHYLENE
METHOD: 4440 , TESTIDCODE: 34501GCM66
Open Data Set

Analysis Date = 12/12/16 SpikeMix = Accu 216041125: 40 µl & Crescent 03FF058: 40 µl Pct Recovery = 93% Analysis Date = 07/20/16 SpikeMix = Supelco LC20141V: 40 µl & Accu 216041125: 40 µl Pct Recovery = 82% Analysis Date = 08/12/16 SpikeMix = ChemService 5082900: 25 µl & Phenova B20160319: 25 µl Pct Recovery = 91% Analysis Date = 06/21/16 SpikeMix = Phenova B20160319: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 97% Analysis Date = 09/08/16 SpikeMix = Supelco LC20141V: 25 µl & Accu 216041125: 25 µl Pct Recovery = 81% Analysis Date = 05/24/16 SpikeMix = Accu 216041125: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 89% Analysis Date = 03/19/15 SpikeMix = Spex Organics C1140417015: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 93% Analysis Date = 12/17/14 SpikeMix = Supelco LC06438: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 76% Analysis Date = 11/14/14 SpikeMix = Crescent 03DD004: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 85% Analysis Date = 06/10/14 SpikeMix = Crescent 03DD004: 20 µl & NSI 032614: 20 µl Pct Recovery = 96% Analysis Date = 09/29/15 SpikeMix = Accu 215041380: 25 µl & ERA 0406-15-03: 25 µl Pct Recovery = 102% Analysis Date = 07/13/15 SpikeMix = Crescent 04EE008: 25 µl & NSI 050515AVOC: 25 µl Pct Recovery = 138% Analysis Date = 06/16/15 SpikeMix = ERA 0406-15-03: 25 µl & Supelco LC13545: 25 µl Pct Recovery = 107% Analysis Date = 04/09/15 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 77% Analysis Date = 08/19/14 SpikeMix = Spex Organics C1140417015: 20 µl & Accu 214031115: 20 µl Pct Recovery = 107% Analysis Date = 07/01/14 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 115% Analysis Date = 05/01/14 SpikeMix = Accu 214031115: 20 µl & NSI 032614: 20 µl Pct Recovery = 93% Analysis Date = 11/29/16 SpikeMix = ChemService 5082900: 15 µl & Phenova B20160319: 15 µl Pct Recovery = 105% Analysis Date = 09/08/16 SpikeMix = Phenova B20160319: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 110% Analysis Date = 05/27/16 SpikeMix = Phenova B20160319: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 97% Analysis Date = 08/20/16 SpikeMix = Accu 216041125: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 96% Analysis Date = 06/30/16 SpikeMix = ChemService 5082900: 15 µl & Accu 216041125: 15 µl Pct Recovery = 68% Analysis Date = 04/26/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 103% Analysis Date = 03/04/16 SpikeMix = Accu 215041380: 15 µl & ERA 0406-15-03: 15 µl Pct Recovery = 109% Analysis Date = 02/05/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 109% Analysis Date = 11/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 118% Analysis Date = 10/17/15 SpikeMix = Crescent 04EE008: 15 µl & NSI 050515AVOC: 15 µl Pct Recovery = 117% Analysis Date = 10/16/15 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 100% Analysis Date = 06/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Accu 215041380: 15 µl Pct Recovery = 126% Analysis Date = 11/06/14 SpikeMix = Spex Organics C1140417015: 10 µl & Crescent 03DD004: 10 µl Pct Recovery = 90% Analysis Date = 10/04/14 SpikeMix = Crescent 03DD004: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 93% Analysis Date = 07/29/14 SpikeMix = Crescent 03DD004: 10 µl & NSI 032614: 10 µl Pct Recovery = 98% Analysis Date = 05/03/14 SpikeMix = Crescent 03DD004: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 93% Analysis Date = 01/13/15 SpikeMix = Accu 214031115: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 98% Analysis Date = 09/09/14 SpikeMix = Accu 214031115: 10 µl & NSI 032614: 10 µl Pct Recovery = 109% Analysis Date = 07/23/14 SpikeMix = Spex Organics C1140417015: 10 µl & Accu 214031115: 10 µl Pct Recovery = 131% Analysis Date = 06/18/14 SpikeMix = Supelco LC06438: 10 µl & Accu 214031115: 10 µl Pct Recovery = 110% Analysis Date = 03/17/16 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 122% Analysis Date = 01/27/16 SpikeMix = Crescent 04EE008: 10 µl & NSI 050515AVOC: 10 µl Pct Recovery = 128% Analysis Date = 12/10/15 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 141% Analysis Date = 11/20/15 SpikeMix = Accu 215041380: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 105% Analysis Date = 09/03/15 SpikeMix = NSI 050515AVOC: 10 µl & Spex Organics EN150428007: 10 µl Pct Recovery = 130% Analysis Date = 07/31/15 SpikeMix = Crescent 04EE008: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 108% Analysis Date = 06/27/15 SpikeMix = ERA 0406-15-03: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 109% Analysis Date = 12/11/16 Pct Recovery = 87% Analysis Date = 12/07/16 Pct Recovery = 87% Analysis Date = 12/07/16 Pct Recovery = 87% Analysis Date = 12/02/16 Pct Recovery = 87% Analysis Date = 12/02/16 Pct Recovery = 87% Analysis Date = 11/27/16 Pct Recovery = 88% Analysis Date = 11/27/16 Pct Recovery = 88% Analysis Date = 11/22/16 Pct Recovery = 88% Analysis Date = 11/22/16 Pct Recovery = 88% Analysis Date = 11/18/16 Pct Recovery = 88% Analysis Date = 11/18/16 Pct Recovery = 88% Analysis Date = 11/13/16 Pct Recovery = 89% Analysis Date = 11/13/16 Pct Recovery = 89% Analysis Date = 11/08/16 Pct Recovery = 89% Analysis Date = 11/08/16 Pct Recovery = 89% Analysis Date = 11/03/16 Pct Recovery = 89% Analysis Date = 11/03/16 Pct Recovery = 89% Analysis Date = 10/29/16 Pct Recovery = 90% Analysis Date = 10/29/16 Pct Recovery = 90% Analysis Date = 10/25/16 Pct Recovery = 90% Analysis Date = 10/25/16 Pct Recovery = 90% Analysis Date = 10/20/16 Pct Recovery = 90% Analysis Date = 10/20/16 Pct Recovery = 90% Analysis Date = 10/15/16 Pct Recovery = 90% Analysis Date = 10/15/16 Pct Recovery = 90% Analysis Date = 10/10/16 Pct Recovery = 91% Analysis Date = 10/10/16 Pct Recovery = 91% Analysis Date = 10/06/16 Pct Recovery = 91% Analysis Date = 10/06/16 Pct Recovery = 91% Analysis Date = 10/01/16 Pct Recovery = 91% Analysis Date = 10/01/16 Pct Recovery = 91% Analysis Date = 09/26/16 Pct Recovery = 92% Analysis Date = 09/26/16 Pct Recovery = 92% Analysis Date = 09/21/16 Pct Recovery = 92% Analysis Date = 09/21/16 Pct Recovery = 92% Analysis Date = 09/16/16 Pct Recovery = 92% Analysis Date = 09/16/16 Pct Recovery = 92% Analysis Date = 09/12/16 Pct Recovery = 93% Analysis Date = 09/12/16 Pct Recovery = 93% Analysis Date = 09/07/16 Pct Recovery = 93% Analysis Date = 09/07/16 Pct Recovery = 93% Analysis Date = 09/02/16 Pct Recovery = 93% Analysis Date = 09/02/16 Pct Recovery = 93% Analysis Date = 08/28/16 Pct Recovery = 94% Analysis Date = 08/28/16 Pct Recovery = 94% Analysis Date = 08/24/16 Pct Recovery = 94% Analysis Date = 08/24/16 Pct Recovery = 94% Analysis Date = 08/19/16 Pct Recovery = 94% Analysis Date = 08/19/16 Pct Recovery = 94% Analysis Date = 08/14/16 Pct Recovery = 95% Analysis Date = 08/14/16 Pct Recovery = 95% Analysis Date = 08/09/16 Pct Recovery = 95% Analysis Date = 08/09/16 Pct Recovery = 95% Analysis Date = 08/04/16 Pct Recovery = 95% Analysis Date = 08/04/16 Pct Recovery = 95% Analysis Date = 07/31/16 Pct Recovery = 96% Analysis Date = 07/31/16 Pct Recovery = 96% Analysis Date = 07/26/16 Pct Recovery = 96% Analysis Date = 07/26/16 Pct Recovery = 96% Analysis Date = 07/21/16 Pct Recovery = 96% Analysis Date = 07/21/16 Pct Recovery = 96% Analysis Date = 07/16/16 Pct Recovery = 97% Analysis Date = 07/16/16 Pct Recovery = 97% Analysis Date = 07/12/16 Pct Recovery = 97% Analysis Date = 07/12/16 Pct Recovery = 97% Analysis Date = 07/07/16 Pct Recovery = 97% Analysis Date = 07/07/16 Pct Recovery = 97% Analysis Date = 07/02/16 Pct Recovery = 98% Analysis Date = 07/02/16 Pct Recovery = 98% Analysis Date = 06/27/16 Pct Recovery = 98% Analysis Date = 06/27/16 Pct Recovery = 98% Analysis Date = 06/22/16 Pct Recovery = 98% Analysis Date = 06/22/16 Pct Recovery = 98% Analysis Date = 06/18/16 Pct Recovery = 99% Analysis Date = 06/18/16 Pct Recovery = 99% Analysis Date = 06/13/16 Pct Recovery = 99% Analysis Date = 06/13/16 Pct Recovery = 99% Analysis Date = 06/08/16 Pct Recovery = 99% Analysis Date = 06/08/16 Pct Recovery = 99% Analysis Date = 06/03/16 Pct Recovery = 100% Analysis Date = 06/03/16 Pct Recovery = 100% Analysis Date = 05/30/16 Pct Recovery = 100% Analysis Date = 05/30/16 Pct Recovery = 100% Analysis Date = 05/25/16 Pct Recovery = 100% Analysis Date = 05/25/16 Pct Recovery = 100% Analysis Date = 05/20/16 Pct Recovery = 100% Analysis Date = 05/20/16 Pct Recovery = 100% Analysis Date = 05/15/16 Pct Recovery = 101% Analysis Date = 05/15/16 Pct Recovery = 101% Analysis Date = 05/10/16 Pct Recovery = 101% Analysis Date = 05/10/16 Pct Recovery = 101% Analysis Date = 05/06/16 Pct Recovery = 101% Analysis Date = 05/06/16 Pct Recovery = 101% Analysis Date = 05/01/16 Pct Recovery = 102% Analysis Date = 05/01/16 Pct Recovery = 102% Analysis Date = 04/26/16 Pct Recovery = 102% Analysis Date = 04/26/16 Pct Recovery = 102% Analysis Date = 04/21/16 Pct Recovery = 102% Analysis Date = 04/21/16 Pct Recovery = 102% Analysis Date = 04/16/16 Pct Recovery = 103% Analysis Date = 04/16/16 Pct Recovery = 103% Analysis Date = 04/12/16 Pct Recovery = 103% Analysis Date = 04/12/16 Pct Recovery = 103% Analysis Date = 04/07/16 Pct Recovery = 104% Analysis Date = 04/07/16 Pct Recovery = 104% Analysis Date = 04/02/16 Pct Recovery = 104% Analysis Date = 04/02/16 Pct Recovery = 104% Analysis Date = 03/28/16 Pct Recovery = 104% Analysis Date = 03/28/16 Pct Recovery = 104% Analysis Date = 03/24/16 Pct Recovery = 105% Analysis Date = 03/24/16 Pct Recovery = 105% Analysis Date = 03/19/16 Pct Recovery = 105% Analysis Date = 03/19/16 Pct Recovery = 105% Analysis Date = 03/14/16 Pct Recovery = 106% Analysis Date = 03/14/16 Pct Recovery = 106% Analysis Date = 03/09/16 Pct Recovery = 106% Analysis Date = 03/09/16 Pct Recovery = 106% Analysis Date = 03/04/16 Pct Recovery = 106% Analysis Date = 03/04/16 Pct Recovery = 106% Analysis Date = 02/29/16 Pct Recovery = 107% Analysis Date = 02/29/16 Pct Recovery = 107% Analysis Date = 02/24/16 Pct Recovery = 107% Analysis Date = 02/24/16 Pct Recovery = 107% Analysis Date = 02/19/16 Pct Recovery = 108% Analysis Date = 02/19/16 Pct Recovery = 108% Analysis Date = 02/14/16 Pct Recovery = 108% Analysis Date = 02/14/16 Pct Recovery = 108% Analysis Date = 02/10/16 Pct Recovery = 108% Analysis Date = 02/10/16 Pct Recovery = 108% Analysis Date = 02/05/16 Pct Recovery = 109% Analysis Date = 02/05/16 Pct Recovery = 109% Analysis Date = 01/31/16 Pct Recovery = 109% Analysis Date = 01/31/16 Pct Recovery = 109% Analysis Date = 01/26/16 Pct Recovery = 109% Analysis Date = 01/26/16 Pct Recovery = 109% Analysis Date = 01/21/16 Pct Recovery = 110% Analysis Date = 01/21/16 Pct Recovery = 110% Analysis Date = 01/17/16 Pct Recovery = 110% Analysis Date = 01/17/16 Pct Recovery = 110% Analysis Date = 01/12/16 Pct Recovery = 111% Analysis Date = 01/12/16 Pct Recovery = 111% Analysis Date = 01/07/16 Pct Recovery = 111% Analysis Date = 01/07/16 Pct Recovery = 111% Analysis Date = 01/02/16 Pct Recovery = 111% Analysis Date = 01/02/16 Pct Recovery = 111% Analysis Date = 12/29/15 Pct Recovery = 112% Analysis Date = 12/29/15 Pct Recovery = 112% Analysis Date = 12/24/15 Pct Recovery = 112% Analysis Date = 12/24/15 Pct Recovery = 112% Analysis Date = 12/19/15 Pct Recovery = 113% Analysis Date = 12/19/15 Pct Recovery = 113% Analysis Date = 12/14/15 Pct Recovery = 113% Analysis Date = 12/14/15 Pct Recovery = 113% Analysis Date = 12/09/15 Pct Recovery = 113% Analysis Date = 12/09/15 Pct Recovery = 113% Analysis Date = 12/05/15 Pct Recovery = 113% Analysis Date = 12/05/15 Pct Recovery = 113% Analysis Date = 11/30/15 Pct Recovery = 114% Analysis Date = 11/30/15 Pct Recovery = 114% Analysis Date = 11/25/15 Pct Recovery = 114% Analysis Date = 11/25/15 Pct Recovery = 114% Analysis Date = 11/20/15 Pct Recovery = 114% Analysis Date = 11/20/15 Pct Recovery = 114% Analysis Date = 11/16/15 Pct Recovery = 114% Analysis Date = 11/16/15 Pct Recovery = 114% Analysis Date = 11/11/15 Pct Recovery = 114% Analysis Date = 11/11/15 Pct Recovery = 114% Analysis Date = 11/06/15 Pct Recovery = 114% Analysis Date = 11/06/15 Pct Recovery = 114% Analysis Date = 11/01/15 Pct Recovery = 114% Analysis Date = 11/01/15 Pct Recovery = 114% Analysis Date = 10/27/15 Pct Recovery = 114% Analysis Date = 10/27/15 Pct Recovery = 114% Analysis Date = 10/23/15 Pct Recovery = 114% Analysis Date = 10/23/15 Pct Recovery = 114% Analysis Date = 10/18/15 Pct Recovery = 114% Analysis Date = 10/18/15 Pct Recovery = 114% Analysis Date = 10/13/15 Pct Recovery = 114% Analysis Date = 10/13/15 Pct Recovery = 114% Analysis Date = 10/08/15 Pct Recovery = 114% Analysis Date = 10/08/15 Pct Recovery = 114% Analysis Date = 10/04/15 Pct Recovery = 114% Analysis Date = 10/04/15 Pct Recovery = 114% Analysis Date = 09/29/15 Pct Recovery = 114% Analysis Date = 09/29/15 Pct Recovery = 114% Analysis Date = 09/24/15 Pct Recovery = 114% Analysis Date = 09/24/15 Pct Recovery = 114% Analysis Date = 09/19/15 Pct Recovery = 113% Analysis Date = 09/19/15 Pct Recovery = 113% Analysis Date = 09/14/15 Pct Recovery = 113% Analysis Date = 09/14/15 Pct Recovery = 113% Analysis Date = 09/10/15 Pct Recovery = 113% Analysis Date = 09/10/15 Pct Recovery = 113% Analysis Date = 09/05/15 Pct Recovery = 113% Analysis Date = 09/05/15 Pct Recovery = 113% Analysis Date = 08/31/15 Pct Recovery = 113% Analysis Date = 08/31/15 Pct Recovery = 113% Analysis Date = 08/26/15 Pct Recovery = 112% Analysis Date = 08/26/15 Pct Recovery = 112% Analysis Date = 08/21/15 Pct Recovery = 112% Analysis Date = 08/21/15 Pct Recovery = 112% Analysis Date = 08/17/15 Pct Recovery = 112% Analysis Date = 08/17/15 Pct Recovery = 112% Analysis Date = 08/12/15 Pct Recovery = 111% Analysis Date = 08/12/15 Pct Recovery = 111% Analysis Date = 08/07/15 Pct Recovery = 111% Analysis Date = 08/07/15 Pct Recovery = 111% Analysis Date = 08/02/15 Pct Recovery = 111% Analysis Date = 08/02/15 Pct Recovery = 111% Analysis Date = 07/29/15 Pct Recovery = 110% Analysis Date = 07/29/15 Pct Recovery = 110% Analysis Date = 07/24/15 Pct Recovery = 110% Analysis Date = 07/24/15 Pct Recovery = 110% Analysis Date = 07/19/15 Pct Recovery = 109% Analysis Date = 07/19/15 Pct Recovery = 109% Analysis Date = 07/14/15 Pct Recovery = 109% Analysis Date = 07/14/15 Pct Recovery = 109% Analysis Date = 07/09/15 Pct Recovery = 109% Analysis Date = 07/09/15 Pct Recovery = 109% Analysis Date = 07/05/15 Pct Recovery = 108% Analysis Date = 07/05/15 Pct Recovery = 108% Analysis Date = 06/30/15 Pct Recovery = 108% Analysis Date = 06/30/15 Pct Recovery = 108% Analysis Date = 06/25/15 Pct Recovery = 108% Analysis Date = 06/25/15 Pct Recovery = 108% Analysis Date = 06/20/15 Pct Recovery = 107% Analysis Date = 06/20/15 Pct Recovery = 107% Analysis Date = 06/16/15 Pct Recovery = 107% Analysis Date = 06/16/15 Pct Recovery = 107% Analysis Date = 06/11/15 Pct Recovery = 106% Analysis Date = 06/11/15 Pct Recovery = 106% Analysis Date = 06/06/15 Pct Recovery = 106% Analysis Date = 06/06/15 Pct Recovery = 106% Analysis Date = 06/01/15 Pct Recovery = 106% Analysis Date = 06/01/15 Pct Recovery = 106% Analysis Date = 05/27/15 Pct Recovery = 106% Analysis Date = 05/27/15 Pct Recovery = 106% Analysis Date = 05/23/15 Pct Recovery = 105% Analysis Date = 05/23/15 Pct Recovery = 105% Analysis Date = 05/18/15 Pct Recovery = 105% Analysis Date = 05/18/15 Pct Recovery = 105% Analysis Date = 05/13/15 Pct Recovery = 105% Analysis Date = 05/13/15 Pct Recovery = 105% Analysis Date = 05/08/15 Pct Recovery = 105% Analysis Date = 05/08/15 Pct Recovery = 105% Analysis Date = 05/04/15 Pct Recovery = 105% Analysis Date = 05/04/15 Pct Recovery = 105% Analysis Date = 04/29/15 Pct Recovery = 104% Analysis Date = 04/29/15 Pct Recovery = 104% Analysis Date = 04/24/15 Pct Recovery = 104% Analysis Date = 04/24/15 Pct Recovery = 104% Analysis Date = 04/19/15 Pct Recovery = 104% Analysis Date = 04/19/15 Pct Recovery = 104% Analysis Date = 04/14/15 Pct Recovery = 104% Analysis Date = 04/14/15 Pct Recovery = 104% Analysis Date = 04/10/15 Pct Recovery = 104% Analysis Date = 04/10/15 Pct Recovery = 104% Analysis Date = 04/05/15 Pct Recovery = 104% Analysis Date = 04/05/15 Pct Recovery = 104% Analysis Date = 03/31/15 Pct Recovery = 103% Analysis Date = 03/31/15 Pct Recovery = 103% Analysis Date = 03/26/15 Pct Recovery = 103% Analysis Date = 03/26/15 Pct Recovery = 103% Analysis Date = 03/22/15 Pct Recovery = 103% Analysis Date = 03/22/15 Pct Recovery = 103% Analysis Date = 03/17/15 Pct Recovery = 103% Analysis Date = 03/17/15 Pct Recovery = 103% Analysis Date = 03/12/15 Pct Recovery = 103% Analysis Date = 03/12/15 Pct Recovery = 103% Analysis Date = 03/07/15 Pct Recovery = 102% Analysis Date = 03/07/15 Pct Recovery = 102% Analysis Date = 03/02/15 Pct Recovery = 102% Analysis Date = 03/02/15 Pct Recovery = 102% Analysis Date = 02/26/15 Pct Recovery = 102% Analysis Date = 02/26/15 Pct Recovery = 102% Analysis Date = 02/21/15 Pct Recovery = 102% Analysis Date = 02/21/15 Pct Recovery = 102% Analysis Date = 02/16/15 Pct Recovery = 102% Analysis Date = 02/16/15 Pct Recovery = 102% Analysis Date = 02/11/15 Pct Recovery = 101% Analysis Date = 02/11/15 Pct Recovery = 101% Analysis Date = 02/07/15 Pct Recovery = 101% Analysis Date = 02/07/15 Pct Recovery = 101% Analysis Date = 02/02/15 Pct Recovery = 101% Analysis Date = 02/02/15 Pct Recovery = 101% Analysis Date = 01/28/15 Pct Recovery = 101% Analysis Date = 01/28/15 Pct Recovery = 101% Analysis Date = 01/23/15 Pct Recovery = 101% Analysis Date = 01/23/15 Pct Recovery = 101% Analysis Date = 01/18/15 Pct Recovery = 101% Analysis Date = 01/18/15 Pct Recovery = 101% Analysis Date = 01/14/15 Pct Recovery = 100% Analysis Date = 01/14/15 Pct Recovery = 100% Analysis Date = 01/09/15 Pct Recovery = 100% Analysis Date = 01/09/15 Pct Recovery = 100% Analysis Date = 01/04/15 Pct Recovery = 100% Analysis Date = 01/04/15 Pct Recovery = 100% Analysis Date = 12/30/14 Pct Recovery = 100% Analysis Date = 12/30/14 Pct Recovery = 100% Analysis Date = 12/25/14 Pct Recovery = 100% Analysis Date = 12/25/14 Pct Recovery = 100% Analysis Date = 12/21/14 Pct Recovery = 100% Analysis Date = 12/21/14 Pct Recovery = 100% Analysis Date = 12/16/14 Pct Recovery = 100% Analysis Date = 12/16/14 Pct Recovery = 100% Analysis Date = 12/11/14 Pct Recovery = 100% Analysis Date = 12/11/14 Pct Recovery = 100% Analysis Date = 12/06/14 Pct Recovery = 100% Analysis Date = 12/06/14 Pct Recovery = 100% Analysis Date = 12/02/14 Pct Recovery = 100% Analysis Date = 12/02/14 Pct Recovery = 100% Analysis Date = 11/27/14 Pct Recovery = 100% Analysis Date = 11/27/14 Pct Recovery = 100% Analysis Date = 11/22/14 Pct Recovery = 100% Analysis Date = 11/22/14 Pct Recovery = 100% Analysis Date = 11/17/14 Pct Recovery = 100% Analysis Date = 11/17/14 Pct Recovery = 100% Analysis Date = 11/12/14 Pct Recovery = 100% Analysis Date = 11/12/14 Pct Recovery = 100% Analysis Date = 11/08/14 Pct Recovery = 100% Analysis Date = 11/08/14 Pct Recovery = 100% Analysis Date = 11/03/14 Pct Recovery = 100% Analysis Date = 11/03/14 Pct Recovery = 100% Analysis Date = 10/29/14 Pct Recovery = 100% Analysis Date = 10/29/14 Pct Recovery = 100% Analysis Date = 10/24/14 Pct Recovery = 100% Analysis Date = 10/24/14 Pct Recovery = 100% Analysis Date = 10/20/14 Pct Recovery = 101% Analysis Date = 10/20/14 Pct Recovery = 101% Analysis Date = 10/15/14 Pct Recovery = 101% Analysis Date = 10/15/14 Pct Recovery = 101% Analysis Date = 10/10/14 Pct Recovery = 101% Analysis Date = 10/10/14 Pct Recovery = 101% Analysis Date = 10/05/14 Pct Recovery = 101% Analysis Date = 10/05/14 Pct Recovery = 101% Analysis Date = 09/30/14 Pct Recovery = 101% Analysis Date = 09/30/14 Pct Recovery = 101% Analysis Date = 09/26/14 Pct Recovery = 101% Analysis Date = 09/26/14 Pct Recovery = 101% Analysis Date = 09/21/14 Pct Recovery = 101% Analysis Date = 09/21/14 Pct Recovery = 101% Analysis Date = 09/16/14 Pct Recovery = 101% Analysis Date = 09/16/14 Pct Recovery = 101% Analysis Date = 09/11/14 Pct Recovery = 101% Analysis Date = 09/11/14 Pct Recovery = 101% Analysis Date = 09/07/14 Pct Recovery = 101% Analysis Date = 09/07/14 Pct Recovery = 101% Analysis Date = 09/02/14 Pct Recovery = 101% Analysis Date = 09/02/14 Pct Recovery = 101% Analysis Date = 08/28/14 Pct Recovery = 101% Analysis Date = 08/28/14 Pct Recovery = 101% Analysis Date = 08/23/14 Pct Recovery = 101% Analysis Date = 08/23/14 Pct Recovery = 101% Analysis Date = 08/18/14 Pct Recovery = 101% Analysis Date = 08/18/14 Pct Recovery = 101% Analysis Date = 08/14/14 Pct Recovery = 101% Analysis Date = 08/14/14 Pct Recovery = 101% Analysis Date = 08/09/14 Pct Recovery = 101% Analysis Date = 08/09/14 Pct Recovery = 101% Analysis Date = 08/04/14 Pct Recovery = 101% Analysis Date = 08/04/14 Pct Recovery = 101% Analysis Date = 07/30/14 Pct Recovery = 101% Analysis Date = 07/30/14 Pct Recovery = 101% Analysis Date = 07/26/14 Pct Recovery = 101% Analysis Date = 07/26/14 Pct Recovery = 101% Analysis Date = 07/21/14 Pct Recovery = 101% Analysis Date = 07/21/14 Pct Recovery = 101% Analysis Date = 07/16/14 Pct Recovery = 101% Analysis Date = 07/16/14 Pct Recovery = 101% Analysis Date = 07/11/14 Pct Recovery = 101% Analysis Date = 07/11/14 Pct Recovery = 101% Analysis Date = 07/06/14 Pct Recovery = 101% Analysis Date = 07/06/14 Pct Recovery = 101% Analysis Date = 07/02/14 Pct Recovery = 101% Analysis Date = 07/02/14 Pct Recovery = 101% Analysis Date = 06/27/14 Pct Recovery = 101% Analysis Date = 06/27/14 Pct Recovery = 101% Analysis Date = 06/22/14 Pct Recovery = 101% Analysis Date = 06/22/14 Pct Recovery = 101% Analysis Date = 06/17/14 Pct Recovery = 102% Analysis Date = 06/17/14 Pct Recovery = 102% Analysis Date = 06/13/14 Pct Recovery = 102% Analysis Date = 06/13/14 Pct Recovery = 102% Analysis Date = 06/08/14 Pct Recovery = 102% Analysis Date = 06/08/14 Pct Recovery = 102% Analysis Date = 06/03/14 Pct Recovery = 102% Analysis Date = 06/03/14 Pct Recovery = 102% Analysis Date = 05/29/14 Pct Recovery = 102% Analysis Date = 05/29/14 Pct Recovery = 102% Analysis Date = 05/24/14 Pct Recovery = 102% Analysis Date = 05/24/14 Pct Recovery = 102% Analysis Date = 05/20/14 Pct Recovery = 102% Analysis Date = 05/20/14 Pct Recovery = 102% Analysis Date = 05/15/14 Pct Recovery = 102% Analysis Date = 05/15/14 Pct Recovery = 102% Analysis Date = 05/10/14 Pct Recovery = 102% Analysis Date = 05/10/14 Pct Recovery = 102% Analysis Date = 05/05/14 Pct Recovery = 102% Analysis Date = 05/05/14 Pct Recovery = 102% Analysis Date = 05/01/14 Pct Recovery = 103% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
1,1-DICHLOROETHYLENE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 44 103% 17% 103% 13%
Total 44 103% 17% 103% 13%

Sample Statistics
1,1-DICHLOROETHYLENE

Characteristic N % % Basis
Plotted 44 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 44 .  
False Negatives 0 0% 0 out of 44
Not Spiked 22 .  
False Positives 0 0% 0 out of 22

BQS OBSP Determination:
1,1-DICHLOROPROPENE
METHOD: 4440 , TESTIDCODE: 77168GCM66
Open Data Set

Analysis Date = 08/04/16 SpikeMix = Crescent 03FF058: 40 µl & Supelco LC20141V: 40 µl Pct Recovery = 98% Analysis Date = 07/20/16 SpikeMix = Supelco LC20141V: 40 µl & Accu 216041125: 40 µl Pct Recovery = 91% Analysis Date = 12/16/16 SpikeMix = NSI 041816AVOC: 40 µl & ChemService 5082900: 40 µl Pct Recovery = 113% Analysis Date = 11/21/16 SpikeMix = Crescent 03FF058: 25 µl & Supelco LC20141V: 25 µl Pct Recovery = 92% Analysis Date = 09/08/16 SpikeMix = Supelco LC20141V: 25 µl & Accu 216041125: 25 µl Pct Recovery = 94% Analysis Date = 08/26/16 SpikeMix = NSI 041816AVOC: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 102% Analysis Date = 08/12/16 SpikeMix = ChemService 5082900: 25 µl & Phenova B20160319: 25 µl Pct Recovery = 98% Analysis Date = 06/30/16 SpikeMix = Crescent 03FF058: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 95% Analysis Date = 04/09/15 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 98% Analysis Date = 08/19/14 SpikeMix = Spex Organics C1140417015: 20 µl & Accu 214031115: 20 µl Pct Recovery = 105% Analysis Date = 07/01/14 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 107% Analysis Date = 05/01/14 SpikeMix = Accu 214031115: 20 µl & NSI 032614: 20 µl Pct Recovery = 94% Analysis Date = 03/19/15 SpikeMix = Spex Organics C1140417015: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 99% Analysis Date = 12/17/14 SpikeMix = Supelco LC06438: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 90% Analysis Date = 11/14/14 SpikeMix = Crescent 03DD004: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 90% Analysis Date = 06/10/14 SpikeMix = Crescent 03DD004: 20 µl & NSI 032614: 20 µl Pct Recovery = 100% Analysis Date = 08/15/15 SpikeMix = Supelco LC13545: 25 µl & Crescent 04EE008: 25 µl Pct Recovery = 73% Analysis Date = 06/16/15 SpikeMix = ERA 0406-15-03: 25 µl & Supelco LC13545: 25 µl Pct Recovery = 71% Analysis Date = 10/13/16 SpikeMix = NSI 041816AVOC: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 115% Analysis Date = 05/27/16 SpikeMix = Phenova B20160319: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 96% Analysis Date = 11/29/16 SpikeMix = ChemService 5082900: 15 µl & Phenova B20160319: 15 µl Pct Recovery = 103% Analysis Date = 09/28/16 SpikeMix = Crescent 03FF058: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 106% Analysis Date = 06/30/16 SpikeMix = ChemService 5082900: 15 µl & Accu 216041125: 15 µl Pct Recovery = 96% Analysis Date = 06/10/16 SpikeMix = NSI 041816AVOC: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 117% Analysis Date = 04/26/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 94% Analysis Date = 02/05/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 98% Analysis Date = 11/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 100% Analysis Date = 10/16/15 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 101% Analysis Date = 05/09/15 SpikeMix = Spex Organics EN150428007: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 102% Analysis Date = 04/02/16 SpikeMix = Supelco LC13545: 15 µl & Accu 215041380: 15 µl Pct Recovery = 73% Analysis Date = 12/18/15 SpikeMix = Supelco LC13545: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 78% Analysis Date = 01/13/15 SpikeMix = Accu 214031115: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 96% Analysis Date = 09/09/14 SpikeMix = Accu 214031115: 10 µl & NSI 032614: 10 µl Pct Recovery = 111% Analysis Date = 07/23/14 SpikeMix = Spex Organics C1140417015: 10 µl & Accu 214031115: 10 µl Pct Recovery = 118% Analysis Date = 06/18/14 SpikeMix = Supelco LC06438: 10 µl & Accu 214031115: 10 µl Pct Recovery = 103% Analysis Date = 11/06/14 SpikeMix = Spex Organics C1140417015: 10 µl & Crescent 03DD004: 10 µl Pct Recovery = 95% Analysis Date = 10/04/14 SpikeMix = Crescent 03DD004: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 90% Analysis Date = 07/29/14 SpikeMix = Crescent 03DD004: 10 µl & NSI 032614: 10 µl Pct Recovery = 101% Analysis Date = 05/03/14 SpikeMix = Crescent 03DD004: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 101% Analysis Date = 02/18/16 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 104% Analysis Date = 11/12/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 111% Analysis Date = 09/03/15 SpikeMix = NSI 050515AVOC: 10 µl & Spex Organics EN150428007: 10 µl Pct Recovery = 96% Analysis Date = 05/21/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 117% Analysis Date = 05/13/16 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 80% Analysis Date = 03/17/16 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 68% Analysis Date = 12/10/15 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 77% Analysis Date = 06/27/15 SpikeMix = ERA 0406-15-03: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 77% Analysis Date = 05/09/15 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 73% Analysis Date = 12/15/16 Pct Recovery = 106% Analysis Date = 12/11/16 Pct Recovery = 105% Analysis Date = 12/11/16 Pct Recovery = 105% Analysis Date = 12/06/16 Pct Recovery = 105% Analysis Date = 12/06/16 Pct Recovery = 105% Analysis Date = 12/01/16 Pct Recovery = 105% Analysis Date = 12/01/16 Pct Recovery = 105% Analysis Date = 11/26/16 Pct Recovery = 104% Analysis Date = 11/26/16 Pct Recovery = 104% Analysis Date = 11/21/16 Pct Recovery = 104% Analysis Date = 11/21/16 Pct Recovery = 104% Analysis Date = 11/17/16 Pct Recovery = 104% Analysis Date = 11/17/16 Pct Recovery = 104% Analysis Date = 11/12/16 Pct Recovery = 104% Analysis Date = 11/12/16 Pct Recovery = 104% Analysis Date = 11/07/16 Pct Recovery = 103% Analysis Date = 11/07/16 Pct Recovery = 103% Analysis Date = 11/02/16 Pct Recovery = 103% Analysis Date = 11/02/16 Pct Recovery = 103% Analysis Date = 10/28/16 Pct Recovery = 103% Analysis Date = 10/28/16 Pct Recovery = 103% Analysis Date = 10/24/16 Pct Recovery = 103% Analysis Date = 10/24/16 Pct Recovery = 103% Analysis Date = 10/19/16 Pct Recovery = 102% Analysis Date = 10/19/16 Pct Recovery = 102% Analysis Date = 10/14/16 Pct Recovery = 102% Analysis Date = 10/14/16 Pct Recovery = 102% Analysis Date = 10/09/16 Pct Recovery = 102% Analysis Date = 10/09/16 Pct Recovery = 102% Analysis Date = 10/04/16 Pct Recovery = 101% Analysis Date = 10/04/16 Pct Recovery = 101% Analysis Date = 09/30/16 Pct Recovery = 101% Analysis Date = 09/30/16 Pct Recovery = 101% Analysis Date = 09/25/16 Pct Recovery = 101% Analysis Date = 09/25/16 Pct Recovery = 101% Analysis Date = 09/20/16 Pct Recovery = 101% Analysis Date = 09/20/16 Pct Recovery = 101% Analysis Date = 09/15/16 Pct Recovery = 100% Analysis Date = 09/15/16 Pct Recovery = 100% Analysis Date = 09/10/16 Pct Recovery = 100% Analysis Date = 09/10/16 Pct Recovery = 100% Analysis Date = 09/06/16 Pct Recovery = 100% Analysis Date = 09/06/16 Pct Recovery = 100% Analysis Date = 09/01/16 Pct Recovery = 100% Analysis Date = 09/01/16 Pct Recovery = 100% Analysis Date = 08/27/16 Pct Recovery = 99% Analysis Date = 08/27/16 Pct Recovery = 99% Analysis Date = 08/22/16 Pct Recovery = 99% Analysis Date = 08/22/16 Pct Recovery = 99% Analysis Date = 08/17/16 Pct Recovery = 99% Analysis Date = 08/17/16 Pct Recovery = 99% Analysis Date = 08/13/16 Pct Recovery = 99% Analysis Date = 08/13/16 Pct Recovery = 99% Analysis Date = 08/08/16 Pct Recovery = 98% Analysis Date = 08/08/16 Pct Recovery = 98% Analysis Date = 08/03/16 Pct Recovery = 98% Analysis Date = 08/03/16 Pct Recovery = 98% Analysis Date = 07/29/16 Pct Recovery = 98% Analysis Date = 07/29/16 Pct Recovery = 98% Analysis Date = 07/24/16 Pct Recovery = 98% Analysis Date = 07/24/16 Pct Recovery = 98% Analysis Date = 07/20/16 Pct Recovery = 97% Analysis Date = 07/20/16 Pct Recovery = 97% Analysis Date = 07/15/16 Pct Recovery = 97% Analysis Date = 07/15/16 Pct Recovery = 97% Analysis Date = 07/10/16 Pct Recovery = 97% Analysis Date = 07/10/16 Pct Recovery = 97% Analysis Date = 07/05/16 Pct Recovery = 97% Analysis Date = 07/05/16 Pct Recovery = 97% Analysis Date = 06/30/16 Pct Recovery = 97% Analysis Date = 06/30/16 Pct Recovery = 97% Analysis Date = 06/26/16 Pct Recovery = 96% Analysis Date = 06/26/16 Pct Recovery = 96% Analysis Date = 06/21/16 Pct Recovery = 96% Analysis Date = 06/21/16 Pct Recovery = 96% Analysis Date = 06/16/16 Pct Recovery = 96% Analysis Date = 06/16/16 Pct Recovery = 96% Analysis Date = 06/11/16 Pct Recovery = 96% Analysis Date = 06/11/16 Pct Recovery = 96% Analysis Date = 06/06/16 Pct Recovery = 95% Analysis Date = 06/06/16 Pct Recovery = 95% Analysis Date = 06/02/16 Pct Recovery = 95% Analysis Date = 06/02/16 Pct Recovery = 95% Analysis Date = 05/28/16 Pct Recovery = 95% Analysis Date = 05/28/16 Pct Recovery = 95% Analysis Date = 05/23/16 Pct Recovery = 95% Analysis Date = 05/23/16 Pct Recovery = 95% Analysis Date = 05/18/16 Pct Recovery = 95% Analysis Date = 05/18/16 Pct Recovery = 95% Analysis Date = 05/13/16 Pct Recovery = 94% Analysis Date = 05/13/16 Pct Recovery = 94% Analysis Date = 05/09/16 Pct Recovery = 94% Analysis Date = 05/09/16 Pct Recovery = 94% Analysis Date = 05/04/16 Pct Recovery = 94% Analysis Date = 05/04/16 Pct Recovery = 94% Analysis Date = 04/29/16 Pct Recovery = 94% Analysis Date = 04/29/16 Pct Recovery = 94% Analysis Date = 04/24/16 Pct Recovery = 94% Analysis Date = 04/24/16 Pct Recovery = 94% Analysis Date = 04/19/16 Pct Recovery = 94% Analysis Date = 04/19/16 Pct Recovery = 94% Analysis Date = 04/15/16 Pct Recovery = 93% Analysis Date = 04/15/16 Pct Recovery = 93% Analysis Date = 04/10/16 Pct Recovery = 93% Analysis Date = 04/10/16 Pct Recovery = 93% Analysis Date = 04/05/16 Pct Recovery = 93% Analysis Date = 04/05/16 Pct Recovery = 93% Analysis Date = 03/31/16 Pct Recovery = 93% Analysis Date = 03/31/16 Pct Recovery = 93% Analysis Date = 03/26/16 Pct Recovery = 93% Analysis Date = 03/26/16 Pct Recovery = 93% Analysis Date = 03/22/16 Pct Recovery = 93% Analysis Date = 03/22/16 Pct Recovery = 93% Analysis Date = 03/17/16 Pct Recovery = 93% Analysis Date = 03/17/16 Pct Recovery = 93% Analysis Date = 03/12/16 Pct Recovery = 92% Analysis Date = 03/12/16 Pct Recovery = 92% Analysis Date = 03/07/16 Pct Recovery = 92% Analysis Date = 03/07/16 Pct Recovery = 92% Analysis Date = 03/02/16 Pct Recovery = 92% Analysis Date = 03/02/16 Pct Recovery = 92% Analysis Date = 02/27/16 Pct Recovery = 92% Analysis Date = 02/27/16 Pct Recovery = 92% Analysis Date = 02/22/16 Pct Recovery = 92% Analysis Date = 02/22/16 Pct Recovery = 92% Analysis Date = 02/17/16 Pct Recovery = 92% Analysis Date = 02/17/16 Pct Recovery = 92% Analysis Date = 02/12/16 Pct Recovery = 92% Analysis Date = 02/12/16 Pct Recovery = 92% Analysis Date = 02/07/16 Pct Recovery = 91% Analysis Date = 02/07/16 Pct Recovery = 91% Analysis Date = 02/03/16 Pct Recovery = 91% Analysis Date = 02/03/16 Pct Recovery = 91% Analysis Date = 01/29/16 Pct Recovery = 91% Analysis Date = 01/29/16 Pct Recovery = 91% Analysis Date = 01/24/16 Pct Recovery = 91% Analysis Date = 01/24/16 Pct Recovery = 91% Analysis Date = 01/19/16 Pct Recovery = 91% Analysis Date = 01/19/16 Pct Recovery = 91% Analysis Date = 01/14/16 Pct Recovery = 91% Analysis Date = 01/14/16 Pct Recovery = 91% Analysis Date = 01/10/16 Pct Recovery = 91% Analysis Date = 01/10/16 Pct Recovery = 91% Analysis Date = 01/05/16 Pct Recovery = 91% Analysis Date = 01/05/16 Pct Recovery = 91% Analysis Date = 12/31/15 Pct Recovery = 90% Analysis Date = 12/31/15 Pct Recovery = 90% Analysis Date = 12/26/15 Pct Recovery = 90% Analysis Date = 12/26/15 Pct Recovery = 90% Analysis Date = 12/21/15 Pct Recovery = 90% Analysis Date = 12/21/15 Pct Recovery = 90% Analysis Date = 12/17/15 Pct Recovery = 90% Analysis Date = 12/17/15 Pct Recovery = 90% Analysis Date = 12/12/15 Pct Recovery = 90% Analysis Date = 12/12/15 Pct Recovery = 90% Analysis Date = 12/07/15 Pct Recovery = 90% Analysis Date = 12/07/15 Pct Recovery = 90% Analysis Date = 12/02/15 Pct Recovery = 90% Analysis Date = 12/02/15 Pct Recovery = 90% Analysis Date = 11/27/15 Pct Recovery = 90% Analysis Date = 11/27/15 Pct Recovery = 90% Analysis Date = 11/23/15 Pct Recovery = 90% Analysis Date = 11/23/15 Pct Recovery = 90% Analysis Date = 11/18/15 Pct Recovery = 90% Analysis Date = 11/18/15 Pct Recovery = 90% Analysis Date = 11/13/15 Pct Recovery = 90% Analysis Date = 11/13/15 Pct Recovery = 90% Analysis Date = 11/08/15 Pct Recovery = 90% Analysis Date = 11/08/15 Pct Recovery = 90% Analysis Date = 11/03/15 Pct Recovery = 90% Analysis Date = 11/03/15 Pct Recovery = 90% Analysis Date = 10/30/15 Pct Recovery = 90% Analysis Date = 10/30/15 Pct Recovery = 90% Analysis Date = 10/25/15 Pct Recovery = 90% Analysis Date = 10/25/15 Pct Recovery = 90% Analysis Date = 10/20/15 Pct Recovery = 90% Analysis Date = 10/20/15 Pct Recovery = 90% Analysis Date = 10/15/15 Pct Recovery = 90% Analysis Date = 10/15/15 Pct Recovery = 90% Analysis Date = 10/10/15 Pct Recovery = 90% Analysis Date = 10/10/15 Pct Recovery = 90% Analysis Date = 10/06/15 Pct Recovery = 90% Analysis Date = 10/06/15 Pct Recovery = 90% Analysis Date = 10/01/15 Pct Recovery = 90% Analysis Date = 10/01/15 Pct Recovery = 90% Analysis Date = 09/26/15 Pct Recovery = 90% Analysis Date = 09/26/15 Pct Recovery = 90% Analysis Date = 09/21/15 Pct Recovery = 90% Analysis Date = 09/21/15 Pct Recovery = 90% Analysis Date = 09/16/15 Pct Recovery = 90% Analysis Date = 09/16/15 Pct Recovery = 90% Analysis Date = 09/12/15 Pct Recovery = 90% Analysis Date = 09/12/15 Pct Recovery = 90% Analysis Date = 09/07/15 Pct Recovery = 91% Analysis Date = 09/07/15 Pct Recovery = 91% Analysis Date = 09/02/15 Pct Recovery = 91% Analysis Date = 09/02/15 Pct Recovery = 91% Analysis Date = 08/28/15 Pct Recovery = 91% Analysis Date = 08/28/15 Pct Recovery = 91% Analysis Date = 08/23/15 Pct Recovery = 91% Analysis Date = 08/23/15 Pct Recovery = 91% Analysis Date = 08/19/15 Pct Recovery = 91% Analysis Date = 08/19/15 Pct Recovery = 91% Analysis Date = 08/14/15 Pct Recovery = 91% Analysis Date = 08/14/15 Pct Recovery = 91% Analysis Date = 08/09/15 Pct Recovery = 91% Analysis Date = 08/09/15 Pct Recovery = 91% Analysis Date = 08/04/15 Pct Recovery = 91% Analysis Date = 08/04/15 Pct Recovery = 91% Analysis Date = 07/30/15 Pct Recovery = 91% Analysis Date = 07/30/15 Pct Recovery = 91% Analysis Date = 07/26/15 Pct Recovery = 91% Analysis Date = 07/26/15 Pct Recovery = 91% Analysis Date = 07/21/15 Pct Recovery = 91% Analysis Date = 07/21/15 Pct Recovery = 91% Analysis Date = 07/16/15 Pct Recovery = 91% Analysis Date = 07/16/15 Pct Recovery = 91% Analysis Date = 07/11/15 Pct Recovery = 91% Analysis Date = 07/11/15 Pct Recovery = 91% Analysis Date = 07/06/15 Pct Recovery = 91% Analysis Date = 07/06/15 Pct Recovery = 91% Analysis Date = 07/02/15 Pct Recovery = 91% Analysis Date = 07/02/15 Pct Recovery = 91% Analysis Date = 06/27/15 Pct Recovery = 92% Analysis Date = 06/27/15 Pct Recovery = 92% Analysis Date = 06/22/15 Pct Recovery = 92% Analysis Date = 06/22/15 Pct Recovery = 92% Analysis Date = 06/17/15 Pct Recovery = 92% Analysis Date = 06/17/15 Pct Recovery = 92% Analysis Date = 06/12/15 Pct Recovery = 92% Analysis Date = 06/12/15 Pct Recovery = 92% Analysis Date = 06/08/15 Pct Recovery = 92% Analysis Date = 06/08/15 Pct Recovery = 92% Analysis Date = 06/03/15 Pct Recovery = 92% Analysis Date = 06/03/15 Pct Recovery = 92% Analysis Date = 05/29/15 Pct Recovery = 92% Analysis Date = 05/29/15 Pct Recovery = 92% Analysis Date = 05/24/15 Pct Recovery = 92% Analysis Date = 05/24/15 Pct Recovery = 92% Analysis Date = 05/19/15 Pct Recovery = 92% Analysis Date = 05/19/15 Pct Recovery = 92% Analysis Date = 05/15/15 Pct Recovery = 92% Analysis Date = 05/15/15 Pct Recovery = 92% Analysis Date = 05/10/15 Pct Recovery = 92% Analysis Date = 05/10/15 Pct Recovery = 92% Analysis Date = 05/05/15 Pct Recovery = 92% Analysis Date = 05/05/15 Pct Recovery = 92% Analysis Date = 04/30/15 Pct Recovery = 92% Analysis Date = 04/30/15 Pct Recovery = 92% Analysis Date = 04/25/15 Pct Recovery = 92% Analysis Date = 04/25/15 Pct Recovery = 92% Analysis Date = 04/21/15 Pct Recovery = 92% Analysis Date = 04/21/15 Pct Recovery = 92% Analysis Date = 04/16/15 Pct Recovery = 93% Analysis Date = 04/16/15 Pct Recovery = 93% Analysis Date = 04/11/15 Pct Recovery = 93% Analysis Date = 04/11/15 Pct Recovery = 93% Analysis Date = 04/06/15 Pct Recovery = 93% Analysis Date = 04/06/15 Pct Recovery = 93% Analysis Date = 04/01/15 Pct Recovery = 93% Analysis Date = 04/01/15 Pct Recovery = 93% Analysis Date = 03/28/15 Pct Recovery = 93% Analysis Date = 03/28/15 Pct Recovery = 93% Analysis Date = 03/23/15 Pct Recovery = 93% Analysis Date = 03/23/15 Pct Recovery = 93% Analysis Date = 03/18/15 Pct Recovery = 93% Analysis Date = 03/18/15 Pct Recovery = 93% Analysis Date = 03/13/15 Pct Recovery = 93% Analysis Date = 03/13/15 Pct Recovery = 93% Analysis Date = 03/08/15 Pct Recovery = 94% Analysis Date = 03/08/15 Pct Recovery = 94% Analysis Date = 03/04/15 Pct Recovery = 94% Analysis Date = 03/04/15 Pct Recovery = 94% Analysis Date = 02/27/15 Pct Recovery = 94% Analysis Date = 02/27/15 Pct Recovery = 94% Analysis Date = 02/22/15 Pct Recovery = 94% Analysis Date = 02/22/15 Pct Recovery = 94% Analysis Date = 02/17/15 Pct Recovery = 94% Analysis Date = 02/17/15 Pct Recovery = 94% Analysis Date = 02/12/15 Pct Recovery = 94% Analysis Date = 02/12/15 Pct Recovery = 94% Analysis Date = 02/08/15 Pct Recovery = 95% Analysis Date = 02/08/15 Pct Recovery = 95% Analysis Date = 02/03/15 Pct Recovery = 95% Analysis Date = 02/03/15 Pct Recovery = 95% Analysis Date = 01/29/15 Pct Recovery = 95% Analysis Date = 01/29/15 Pct Recovery = 95% Analysis Date = 01/24/15 Pct Recovery = 95% Analysis Date = 01/24/15 Pct Recovery = 95% Analysis Date = 01/19/15 Pct Recovery = 95% Analysis Date = 01/19/15 Pct Recovery = 95% Analysis Date = 01/15/15 Pct Recovery = 95% Analysis Date = 01/15/15 Pct Recovery = 95% Analysis Date = 01/10/15 Pct Recovery = 96% Analysis Date = 01/10/15 Pct Recovery = 96% Analysis Date = 01/05/15 Pct Recovery = 96% Analysis Date = 01/05/15 Pct Recovery = 96% Analysis Date = 12/31/14 Pct Recovery = 96% Analysis Date = 12/31/14 Pct Recovery = 96% Analysis Date = 12/26/14 Pct Recovery = 96% Analysis Date = 12/26/14 Pct Recovery = 96% Analysis Date = 12/22/14 Pct Recovery = 96% Analysis Date = 12/22/14 Pct Recovery = 96% Analysis Date = 12/17/14 Pct Recovery = 97% Analysis Date = 12/17/14 Pct Recovery = 97% Analysis Date = 12/12/14 Pct Recovery = 97% Analysis Date = 12/12/14 Pct Recovery = 97% Analysis Date = 12/07/14 Pct Recovery = 97% Analysis Date = 12/07/14 Pct Recovery = 97% Analysis Date = 12/02/14 Pct Recovery = 97% Analysis Date = 12/02/14 Pct Recovery = 97% Analysis Date = 11/28/14 Pct Recovery = 97% Analysis Date = 11/28/14 Pct Recovery = 97% Analysis Date = 11/23/14 Pct Recovery = 97% Analysis Date = 11/23/14 Pct Recovery = 97% Analysis Date = 11/18/14 Pct Recovery = 98% Analysis Date = 11/18/14 Pct Recovery = 98% Analysis Date = 11/13/14 Pct Recovery = 98% Analysis Date = 11/13/14 Pct Recovery = 98% Analysis Date = 11/08/14 Pct Recovery = 98% Analysis Date = 11/08/14 Pct Recovery = 98% Analysis Date = 11/04/14 Pct Recovery = 98% Analysis Date = 11/04/14 Pct Recovery = 98% Analysis Date = 10/30/14 Pct Recovery = 98% Analysis Date = 10/30/14 Pct Recovery = 98% Analysis Date = 10/25/14 Pct Recovery = 98% Analysis Date = 10/25/14 Pct Recovery = 98% Analysis Date = 10/20/14 Pct Recovery = 99% Analysis Date = 10/20/14 Pct Recovery = 99% Analysis Date = 10/15/14 Pct Recovery = 99% Analysis Date = 10/15/14 Pct Recovery = 99% Analysis Date = 10/11/14 Pct Recovery = 99% Analysis Date = 10/11/14 Pct Recovery = 99% Analysis Date = 10/06/14 Pct Recovery = 99% Analysis Date = 10/06/14 Pct Recovery = 99% Analysis Date = 10/01/14 Pct Recovery = 99% Analysis Date = 10/01/14 Pct Recovery = 99% Analysis Date = 09/26/14 Pct Recovery = 99% Analysis Date = 09/26/14 Pct Recovery = 99% Analysis Date = 09/21/14 Pct Recovery = 100% Analysis Date = 09/21/14 Pct Recovery = 100% Analysis Date = 09/17/14 Pct Recovery = 100% Analysis Date = 09/17/14 Pct Recovery = 100% Analysis Date = 09/12/14 Pct Recovery = 100% Analysis Date = 09/12/14 Pct Recovery = 100% Analysis Date = 09/07/14 Pct Recovery = 100% Analysis Date = 09/07/14 Pct Recovery = 100% Analysis Date = 09/02/14 Pct Recovery = 100% Analysis Date = 09/02/14 Pct Recovery = 100% Analysis Date = 08/28/14 Pct Recovery = 100% Analysis Date = 08/28/14 Pct Recovery = 100% Analysis Date = 08/24/14 Pct Recovery = 101% Analysis Date = 08/24/14 Pct Recovery = 101% Analysis Date = 08/19/14 Pct Recovery = 101% Analysis Date = 08/19/14 Pct Recovery = 101% Analysis Date = 08/14/14 Pct Recovery = 101% Analysis Date = 08/14/14 Pct Recovery = 101% Analysis Date = 08/09/14 Pct Recovery = 101% Analysis Date = 08/09/14 Pct Recovery = 101% Analysis Date = 08/04/14 Pct Recovery = 101% Analysis Date = 08/04/14 Pct Recovery = 101% Analysis Date = 07/31/14 Pct Recovery = 101% Analysis Date = 07/31/14 Pct Recovery = 101% Analysis Date = 07/26/14 Pct Recovery = 102% Analysis Date = 07/26/14 Pct Recovery = 102% Analysis Date = 07/21/14 Pct Recovery = 102% Analysis Date = 07/21/14 Pct Recovery = 102% Analysis Date = 07/16/14 Pct Recovery = 102% Analysis Date = 07/16/14 Pct Recovery = 102% Analysis Date = 07/11/14 Pct Recovery = 102% Analysis Date = 07/11/14 Pct Recovery = 102% Analysis Date = 07/07/14 Pct Recovery = 102% Analysis Date = 07/07/14 Pct Recovery = 102% Analysis Date = 07/02/14 Pct Recovery = 102% Analysis Date = 07/02/14 Pct Recovery = 102% Analysis Date = 06/27/14 Pct Recovery = 103% Analysis Date = 06/27/14 Pct Recovery = 103% Analysis Date = 06/22/14 Pct Recovery = 103% Analysis Date = 06/22/14 Pct Recovery = 103% Analysis Date = 06/17/14 Pct Recovery = 103% Analysis Date = 06/17/14 Pct Recovery = 103% Analysis Date = 06/13/14 Pct Recovery = 103% Analysis Date = 06/13/14 Pct Recovery = 103% Analysis Date = 06/08/14 Pct Recovery = 103% Analysis Date = 06/08/14 Pct Recovery = 103% Analysis Date = 06/03/14 Pct Recovery = 103% Analysis Date = 06/03/14 Pct Recovery = 103% Analysis Date = 05/29/14 Pct Recovery = 104% Analysis Date = 05/29/14 Pct Recovery = 104% Analysis Date = 05/24/14 Pct Recovery = 104% Analysis Date = 05/24/14 Pct Recovery = 104% Analysis Date = 05/20/14 Pct Recovery = 104% Analysis Date = 05/20/14 Pct Recovery = 104% Analysis Date = 05/15/14 Pct Recovery = 104% Analysis Date = 05/15/14 Pct Recovery = 104% Analysis Date = 05/10/14 Pct Recovery = 104% Analysis Date = 05/10/14 Pct Recovery = 104% Analysis Date = 05/05/14 Pct Recovery = 105% Analysis Date = 05/05/14 Pct Recovery = 105% Analysis Date = 05/01/14 Pct Recovery = 105% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
1,1-DICHLOROPROPENE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 48 96% 13% 98% 9%
Total 48 96% 13% 98% 9%

Sample Statistics
1,1-DICHLOROPROPENE

Characteristic N % % Basis
Plotted 48 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 48 .  
False Negatives 0 0% 0 out of 48
Not Spiked 25 .  
False Positives 1 4% 1 out of 25

BQS OBSP Determination:
1,1-DIFLUOROETHANE
METHOD: 4440 , TESTIDCODE: 49538GCM66
Open Data Set

Analysis Date = 12/12/16 SpikeMix = Accu 216041125: 40 µl & Crescent 03FF058: 40 µl Pct Recovery = 74% Analysis Date = 08/04/16 SpikeMix = Crescent 03FF058: 40 µl & Supelco LC20141V: 40 µl Pct Recovery = 71% Analysis Date = 11/21/16 SpikeMix = Crescent 03FF058: 25 µl & Supelco LC20141V: 25 µl Pct Recovery = 60% Analysis Date = 07/06/16 SpikeMix = Crescent 03FF058: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 68% Analysis Date = 06/21/16 SpikeMix = Phenova B20160319: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 65% Analysis Date = 05/24/16 SpikeMix = Accu 216041125: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 64% Analysis Date = 03/19/15 SpikeMix = Spex Organics C1140417015: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 127% Analysis Date = 03/06/15 SpikeMix = ERA 0227-14-06.1A: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 98% Analysis Date = 12/17/14 SpikeMix = Supelco LC06438: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 89% Analysis Date = 11/22/14 SpikeMix = NSI 032614: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 118% Analysis Date = 09/21/14 SpikeMix = Supelco LC06438: 20 µl Pct Recovery = 106% Analysis Date = 08/19/14 SpikeMix = Spex Organics C1140417015: 20 µl & Accu 214031115: 20 µl Pct Recovery = 133% Analysis Date = 08/16/14 SpikeMix = ERA 0227-14-06.1A: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 134% Analysis Date = 06/10/14 SpikeMix = NSI 032614: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 96% Analysis Date = 08/15/15 SpikeMix = Supelco LC13545: 25 µl & Crescent 04EE008: 25 µl Pct Recovery = 117% Analysis Date = 06/16/15 SpikeMix = ERA 0406-15-03: 25 µl & Supelco LC13545: 25 µl Pct Recovery = 106% Analysis Date = 09/28/16 SpikeMix = Crescent 03FF058: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 60% Analysis Date = 09/08/16 SpikeMix = Phenova B20160319: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 69% Analysis Date = 08/20/16 SpikeMix = Accu 216041125: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 65% Analysis Date = 04/26/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 89% Analysis Date = 02/05/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 105% Analysis Date = 11/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 101% Analysis Date = 10/16/15 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 96% Analysis Date = 05/09/15 SpikeMix = Spex Organics EN150428007: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 115% Analysis Date = 04/02/16 SpikeMix = Supelco LC13545: 15 µl & Accu 215041380: 15 µl Pct Recovery = 109% Analysis Date = 12/18/15 SpikeMix = Supelco LC13545: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 106% Analysis Date = 11/06/14 SpikeMix = Spex Organics C1140417015: 10 µl & Crescent 03DD004: 10 µl Pct Recovery = 124% Analysis Date = 10/21/14 SpikeMix = ERA 0227-14-06.1A: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 101% Analysis Date = 09/09/14 SpikeMix = NSI 032614: 10 µl & Spex Organics C1140417015: 10 µl Pct Recovery = 130% Analysis Date = 07/23/14 SpikeMix = Spex Organics C1140417015: 10 µl & Accu 214031115: 10 µl Pct Recovery = 143% Analysis Date = 07/11/14 SpikeMix = Spex Organics C1140417015: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 123% Analysis Date = 06/18/14 SpikeMix = Supelco LC06438: 10 µl & Accu 214031115: 10 µl Pct Recovery = 110% Analysis Date = 05/30/14 SpikeMix = NSI 032614: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 105% Analysis Date = 05/03/14 SpikeMix = Crescent 03DD004: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 105% Analysis Date = 02/18/16 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 100% Analysis Date = 11/12/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 107% Analysis Date = 09/03/15 SpikeMix = NSI 050515AVOC: 10 µl & Spex Organics EN150428007: 10 µl Pct Recovery = 99% Analysis Date = 05/21/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 117% Analysis Date = 05/13/16 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 80% Analysis Date = 03/17/16 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 94% Analysis Date = 12/10/15 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 100% Analysis Date = 06/27/15 SpikeMix = ERA 0406-15-03: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 117% Analysis Date = 05/09/15 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 139% Analysis Date = 12/12/16 Pct Recovery = 57% Analysis Date = 12/07/16 Pct Recovery = 58% Analysis Date = 12/07/16 Pct Recovery = 58% Analysis Date = 12/02/16 Pct Recovery = 58% Analysis Date = 12/02/16 Pct Recovery = 58% Analysis Date = 11/27/16 Pct Recovery = 59% Analysis Date = 11/27/16 Pct Recovery = 59% Analysis Date = 11/22/16 Pct Recovery = 59% Analysis Date = 11/22/16 Pct Recovery = 59% Analysis Date = 11/18/16 Pct Recovery = 60% Analysis Date = 11/18/16 Pct Recovery = 60% Analysis Date = 11/13/16 Pct Recovery = 60% Analysis Date = 11/13/16 Pct Recovery = 60% Analysis Date = 11/08/16 Pct Recovery = 61% Analysis Date = 11/08/16 Pct Recovery = 61% Analysis Date = 11/03/16 Pct Recovery = 62% Analysis Date = 11/03/16 Pct Recovery = 62% Analysis Date = 10/30/16 Pct Recovery = 62% Analysis Date = 10/30/16 Pct Recovery = 62% Analysis Date = 10/25/16 Pct Recovery = 63% Analysis Date = 10/25/16 Pct Recovery = 63% Analysis Date = 10/20/16 Pct Recovery = 63% Analysis Date = 10/20/16 Pct Recovery = 63% Analysis Date = 10/15/16 Pct Recovery = 64% Analysis Date = 10/15/16 Pct Recovery = 64% Analysis Date = 10/10/16 Pct Recovery = 64% Analysis Date = 10/10/16 Pct Recovery = 64% Analysis Date = 10/06/16 Pct Recovery = 65% Analysis Date = 10/06/16 Pct Recovery = 65% Analysis Date = 10/01/16 Pct Recovery = 66% Analysis Date = 10/01/16 Pct Recovery = 66% Analysis Date = 09/26/16 Pct Recovery = 66% Analysis Date = 09/26/16 Pct Recovery = 66% Analysis Date = 09/21/16 Pct Recovery = 67% Analysis Date = 09/21/16 Pct Recovery = 67% Analysis Date = 09/17/16 Pct Recovery = 67% Analysis Date = 09/17/16 Pct Recovery = 67% Analysis Date = 09/12/16 Pct Recovery = 68% Analysis Date = 09/12/16 Pct Recovery = 68% Analysis Date = 09/07/16 Pct Recovery = 68% Analysis Date = 09/07/16 Pct Recovery = 68% Analysis Date = 09/02/16 Pct Recovery = 69% Analysis Date = 09/02/16 Pct Recovery = 69% Analysis Date = 08/29/16 Pct Recovery = 70% Analysis Date = 08/29/16 Pct Recovery = 70% Analysis Date = 08/24/16 Pct Recovery = 70% Analysis Date = 08/24/16 Pct Recovery = 70% Analysis Date = 08/19/16 Pct Recovery = 71% Analysis Date = 08/19/16 Pct Recovery = 71% Analysis Date = 08/14/16 Pct Recovery = 71% Analysis Date = 08/14/16 Pct Recovery = 71% Analysis Date = 08/09/16 Pct Recovery = 72% Analysis Date = 08/09/16 Pct Recovery = 72% Analysis Date = 08/05/16 Pct Recovery = 72% Analysis Date = 08/05/16 Pct Recovery = 72% Analysis Date = 07/31/16 Pct Recovery = 73% Analysis Date = 07/31/16 Pct Recovery = 73% Analysis Date = 07/26/16 Pct Recovery = 73% Analysis Date = 07/26/16 Pct Recovery = 73% Analysis Date = 07/21/16 Pct Recovery = 74% Analysis Date = 07/21/16 Pct Recovery = 74% Analysis Date = 07/17/16 Pct Recovery = 75% Analysis Date = 07/17/16 Pct Recovery = 75% Analysis Date = 07/12/16 Pct Recovery = 75% Analysis Date = 07/12/16 Pct Recovery = 75% Analysis Date = 07/07/16 Pct Recovery = 76% Analysis Date = 07/07/16 Pct Recovery = 76% Analysis Date = 07/02/16 Pct Recovery = 76% Analysis Date = 07/02/16 Pct Recovery = 76% Analysis Date = 06/28/16 Pct Recovery = 77% Analysis Date = 06/28/16 Pct Recovery = 77% Analysis Date = 06/23/16 Pct Recovery = 77% Analysis Date = 06/23/16 Pct Recovery = 77% Analysis Date = 06/18/16 Pct Recovery = 78% Analysis Date = 06/18/16 Pct Recovery = 78% Analysis Date = 06/13/16 Pct Recovery = 78% Analysis Date = 06/13/16 Pct Recovery = 78% Analysis Date = 06/08/16 Pct Recovery = 79% Analysis Date = 06/08/16 Pct Recovery = 79% Analysis Date = 06/04/16 Pct Recovery = 80% Analysis Date = 06/04/16 Pct Recovery = 80% Analysis Date = 05/30/16 Pct Recovery = 80% Analysis Date = 05/30/16 Pct Recovery = 80% Analysis Date = 05/25/16 Pct Recovery = 81% Analysis Date = 05/25/16 Pct Recovery = 81% Analysis Date = 05/20/16 Pct Recovery = 81% Analysis Date = 05/20/16 Pct Recovery = 81% Analysis Date = 05/16/16 Pct Recovery = 82% Analysis Date = 05/16/16 Pct Recovery = 82% Analysis Date = 05/11/16 Pct Recovery = 82% Analysis Date = 05/11/16 Pct Recovery = 82% Analysis Date = 05/06/16 Pct Recovery = 83% Analysis Date = 05/06/16 Pct Recovery = 83% Analysis Date = 05/01/16 Pct Recovery = 83% Analysis Date = 05/01/16 Pct Recovery = 83% Analysis Date = 04/27/16 Pct Recovery = 84% Analysis Date = 04/27/16 Pct Recovery = 84% Analysis Date = 04/22/16 Pct Recovery = 85% Analysis Date = 04/22/16 Pct Recovery = 85% Analysis Date = 04/17/16 Pct Recovery = 85% Analysis Date = 04/17/16 Pct Recovery = 85% Analysis Date = 04/12/16 Pct Recovery = 86% Analysis Date = 04/12/16 Pct Recovery = 86% Analysis Date = 04/07/16 Pct Recovery = 86% Analysis Date = 04/07/16 Pct Recovery = 86% Analysis Date = 04/03/16 Pct Recovery = 87% Analysis Date = 04/03/16 Pct Recovery = 87% Analysis Date = 03/29/16 Pct Recovery = 87% Analysis Date = 03/29/16 Pct Recovery = 87% Analysis Date = 03/24/16 Pct Recovery = 88% Analysis Date = 03/24/16 Pct Recovery = 88% Analysis Date = 03/19/16 Pct Recovery = 89% Analysis Date = 03/19/16 Pct Recovery = 89% Analysis Date = 03/15/16 Pct Recovery = 89% Analysis Date = 03/15/16 Pct Recovery = 89% Analysis Date = 03/10/16 Pct Recovery = 90% Analysis Date = 03/10/16 Pct Recovery = 90% Analysis Date = 03/05/16 Pct Recovery = 90% Analysis Date = 03/05/16 Pct Recovery = 90% Analysis Date = 02/29/16 Pct Recovery = 91% Analysis Date = 02/29/16 Pct Recovery = 91% Analysis Date = 02/25/16 Pct Recovery = 91% Analysis Date = 02/25/16 Pct Recovery = 91% Analysis Date = 02/20/16 Pct Recovery = 92% Analysis Date = 02/20/16 Pct Recovery = 92% Analysis Date = 02/15/16 Pct Recovery = 93% Analysis Date = 02/15/16 Pct Recovery = 93% Analysis Date = 02/10/16 Pct Recovery = 93% Analysis Date = 02/10/16 Pct Recovery = 93% Analysis Date = 02/05/16 Pct Recovery = 94% Analysis Date = 02/05/16 Pct Recovery = 94% Analysis Date = 02/01/16 Pct Recovery = 94% Analysis Date = 02/01/16 Pct Recovery = 94% Analysis Date = 01/27/16 Pct Recovery = 95% Analysis Date = 01/27/16 Pct Recovery = 95% Analysis Date = 01/22/16 Pct Recovery = 95% Analysis Date = 01/22/16 Pct Recovery = 95% Analysis Date = 01/17/16 Pct Recovery = 96% Analysis Date = 01/17/16 Pct Recovery = 96% Analysis Date = 01/13/16 Pct Recovery = 97% Analysis Date = 01/13/16 Pct Recovery = 97% Analysis Date = 01/08/16 Pct Recovery = 97% Analysis Date = 01/08/16 Pct Recovery = 97% Analysis Date = 01/03/16 Pct Recovery = 98% Analysis Date = 01/03/16 Pct Recovery = 98% Analysis Date = 12/29/15 Pct Recovery = 98% Analysis Date = 12/29/15 Pct Recovery = 98% Analysis Date = 12/25/15 Pct Recovery = 99% Analysis Date = 12/25/15 Pct Recovery = 99% Analysis Date = 12/20/15 Pct Recovery = 99% Analysis Date = 12/20/15 Pct Recovery = 99% Analysis Date = 12/15/15 Pct Recovery = 100% Analysis Date = 12/15/15 Pct Recovery = 100% Analysis Date = 12/10/15 Pct Recovery = 100% Analysis Date = 12/10/15 Pct Recovery = 100% Analysis Date = 12/05/15 Pct Recovery = 101% Analysis Date = 12/05/15 Pct Recovery = 101% Analysis Date = 12/01/15 Pct Recovery = 101% Analysis Date = 12/01/15 Pct Recovery = 101% Analysis Date = 11/26/15 Pct Recovery = 102% Analysis Date = 11/26/15 Pct Recovery = 102% Analysis Date = 11/21/15 Pct Recovery = 102% Analysis Date = 11/21/15 Pct Recovery = 102% Analysis Date = 11/16/15 Pct Recovery = 103% Analysis Date = 11/16/15 Pct Recovery = 103% Analysis Date = 11/12/15 Pct Recovery = 103% Analysis Date = 11/12/15 Pct Recovery = 103% Analysis Date = 11/07/15 Pct Recovery = 104% Analysis Date = 11/07/15 Pct Recovery = 104% Analysis Date = 11/02/15 Pct Recovery = 104% Analysis Date = 11/02/15 Pct Recovery = 104% Analysis Date = 10/28/15 Pct Recovery = 104% Analysis Date = 10/28/15 Pct Recovery = 104% Analysis Date = 10/24/15 Pct Recovery = 105% Analysis Date = 10/24/15 Pct Recovery = 105% Analysis Date = 10/19/15 Pct Recovery = 105% Analysis Date = 10/19/15 Pct Recovery = 105% Analysis Date = 10/14/15 Pct Recovery = 105% Analysis Date = 10/14/15 Pct Recovery = 105% Analysis Date = 10/09/15 Pct Recovery = 106% Analysis Date = 10/09/15 Pct Recovery = 106% Analysis Date = 10/04/15 Pct Recovery = 106% Analysis Date = 10/04/15 Pct Recovery = 106% Analysis Date = 09/30/15 Pct Recovery = 106% Analysis Date = 09/30/15 Pct Recovery = 106% Analysis Date = 09/25/15 Pct Recovery = 107% Analysis Date = 09/25/15 Pct Recovery = 107% Analysis Date = 09/20/15 Pct Recovery = 107% Analysis Date = 09/20/15 Pct Recovery = 107% Analysis Date = 09/15/15 Pct Recovery = 107% Analysis Date = 09/15/15 Pct Recovery = 107% Analysis Date = 09/11/15 Pct Recovery = 108% Analysis Date = 09/11/15 Pct Recovery = 108% Analysis Date = 09/06/15 Pct Recovery = 108% Analysis Date = 09/06/15 Pct Recovery = 108% Analysis Date = 09/01/15 Pct Recovery = 108% Analysis Date = 09/01/15 Pct Recovery = 108% Analysis Date = 08/27/15 Pct Recovery = 109% Analysis Date = 08/27/15 Pct Recovery = 109% Analysis Date = 08/23/15 Pct Recovery = 109% Analysis Date = 08/23/15 Pct Recovery = 109% Analysis Date = 08/18/15 Pct Recovery = 109% Analysis Date = 08/18/15 Pct Recovery = 109% Analysis Date = 08/13/15 Pct Recovery = 110% Analysis Date = 08/13/15 Pct Recovery = 110% Analysis Date = 08/08/15 Pct Recovery = 110% Analysis Date = 08/08/15 Pct Recovery = 110% Analysis Date = 08/03/15 Pct Recovery = 110% Analysis Date = 08/03/15 Pct Recovery = 110% Analysis Date = 07/30/15 Pct Recovery = 110% Analysis Date = 07/30/15 Pct Recovery = 110% Analysis Date = 07/25/15 Pct Recovery = 110% Analysis Date = 07/25/15 Pct Recovery = 110% Analysis Date = 07/20/15 Pct Recovery = 110% Analysis Date = 07/20/15 Pct Recovery = 110% Analysis Date = 07/15/15 Pct Recovery = 110% Analysis Date = 07/15/15 Pct Recovery = 110% Analysis Date = 07/11/15 Pct Recovery = 110% Analysis Date = 07/11/15 Pct Recovery = 110% Analysis Date = 07/06/15 Pct Recovery = 111% Analysis Date = 07/06/15 Pct Recovery = 111% Analysis Date = 07/01/15 Pct Recovery = 111% Analysis Date = 07/01/15 Pct Recovery = 111% Analysis Date = 06/26/15 Pct Recovery = 111% Analysis Date = 06/26/15 Pct Recovery = 111% Analysis Date = 06/21/15 Pct Recovery = 111% Analysis Date = 06/21/15 Pct Recovery = 111% Analysis Date = 06/17/15 Pct Recovery = 111% Analysis Date = 06/17/15 Pct Recovery = 111% Analysis Date = 06/12/15 Pct Recovery = 111% Analysis Date = 06/12/15 Pct Recovery = 111% Analysis Date = 06/07/15 Pct Recovery = 111% Analysis Date = 06/07/15 Pct Recovery = 111% Analysis Date = 06/02/15 Pct Recovery = 111% Analysis Date = 06/02/15 Pct Recovery = 111% Analysis Date = 05/29/15 Pct Recovery = 112% Analysis Date = 05/29/15 Pct Recovery = 112% Analysis Date = 05/24/15 Pct Recovery = 112% Analysis Date = 05/24/15 Pct Recovery = 112% Analysis Date = 05/19/15 Pct Recovery = 112% Analysis Date = 05/19/15 Pct Recovery = 112% Analysis Date = 05/14/15 Pct Recovery = 112% Analysis Date = 05/14/15 Pct Recovery = 112% Analysis Date = 05/10/15 Pct Recovery = 112% Analysis Date = 05/10/15 Pct Recovery = 112% Analysis Date = 05/05/15 Pct Recovery = 112% Analysis Date = 05/05/15 Pct Recovery = 112% Analysis Date = 04/30/15 Pct Recovery = 112% Analysis Date = 04/30/15 Pct Recovery = 112% Analysis Date = 04/25/15 Pct Recovery = 112% Analysis Date = 04/25/15 Pct Recovery = 112% Analysis Date = 04/20/15 Pct Recovery = 113% Analysis Date = 04/20/15 Pct Recovery = 113% Analysis Date = 04/16/15 Pct Recovery = 113% Analysis Date = 04/16/15 Pct Recovery = 113% Analysis Date = 04/11/15 Pct Recovery = 113% Analysis Date = 04/11/15 Pct Recovery = 113% Analysis Date = 04/06/15 Pct Recovery = 113% Analysis Date = 04/06/15 Pct Recovery = 113% Analysis Date = 04/01/15 Pct Recovery = 113% Analysis Date = 04/01/15 Pct Recovery = 113% Analysis Date = 03/28/15 Pct Recovery = 113% Analysis Date = 03/28/15 Pct Recovery = 113% Analysis Date = 03/23/15 Pct Recovery = 113% Analysis Date = 03/23/15 Pct Recovery = 113% Analysis Date = 03/18/15 Pct Recovery = 114% Analysis Date = 03/18/15 Pct Recovery = 114% Analysis Date = 03/13/15 Pct Recovery = 114% Analysis Date = 03/13/15 Pct Recovery = 114% Analysis Date = 03/09/15 Pct Recovery = 114% Analysis Date = 03/09/15 Pct Recovery = 114% Analysis Date = 03/04/15 Pct Recovery = 114% Analysis Date = 03/04/15 Pct Recovery = 114% Analysis Date = 02/27/15 Pct Recovery = 114% Analysis Date = 02/27/15 Pct Recovery = 114% Analysis Date = 02/22/15 Pct Recovery = 114% Analysis Date = 02/22/15 Pct Recovery = 114% Analysis Date = 02/17/15 Pct Recovery = 114% Analysis Date = 02/17/15 Pct Recovery = 114% Analysis Date = 02/13/15 Pct Recovery = 115% Analysis Date = 02/13/15 Pct Recovery = 115% Analysis Date = 02/08/15 Pct Recovery = 115% Analysis Date = 02/08/15 Pct Recovery = 115% Analysis Date = 02/03/15 Pct Recovery = 115% Analysis Date = 02/03/15 Pct Recovery = 115% Analysis Date = 01/29/15 Pct Recovery = 115% Analysis Date = 01/29/15 Pct Recovery = 115% Analysis Date = 01/25/15 Pct Recovery = 115% Analysis Date = 01/25/15 Pct Recovery = 115% Analysis Date = 01/20/15 Pct Recovery = 115% Analysis Date = 01/20/15 Pct Recovery = 115% Analysis Date = 01/15/15 Pct Recovery = 115% Analysis Date = 01/15/15 Pct Recovery = 115% Analysis Date = 01/10/15 Pct Recovery = 116% Analysis Date = 01/10/15 Pct Recovery = 116% Analysis Date = 01/06/15 Pct Recovery = 116% Analysis Date = 01/06/15 Pct Recovery = 116% Analysis Date = 01/01/15 Pct Recovery = 116% Analysis Date = 01/01/15 Pct Recovery = 116% Analysis Date = 12/27/14 Pct Recovery = 116% Analysis Date = 12/27/14 Pct Recovery = 116% Analysis Date = 12/22/14 Pct Recovery = 116% Analysis Date = 12/22/14 Pct Recovery = 116% Analysis Date = 12/17/14 Pct Recovery = 116% Analysis Date = 12/17/14 Pct Recovery = 116% Analysis Date = 12/13/14 Pct Recovery = 116% Analysis Date = 12/13/14 Pct Recovery = 116% Analysis Date = 12/08/14 Pct Recovery = 116% Analysis Date = 12/08/14 Pct Recovery = 116% Analysis Date = 12/03/14 Pct Recovery = 116% Analysis Date = 12/03/14 Pct Recovery = 116% Analysis Date = 11/28/14 Pct Recovery = 116% Analysis Date = 11/28/14 Pct Recovery = 116% Analysis Date = 11/24/14 Pct Recovery = 116% Analysis Date = 11/24/14 Pct Recovery = 116% Analysis Date = 11/19/14 Pct Recovery = 116% Analysis Date = 11/19/14 Pct Recovery = 116% Analysis Date = 11/14/14 Pct Recovery = 116% Analysis Date = 11/14/14 Pct Recovery = 116% Analysis Date = 11/09/14 Pct Recovery = 116% Analysis Date = 11/09/14 Pct Recovery = 116% Analysis Date = 11/05/14 Pct Recovery = 116% Analysis Date = 11/05/14 Pct Recovery = 116% Analysis Date = 10/31/14 Pct Recovery = 116% Analysis Date = 10/31/14 Pct Recovery = 116% Analysis Date = 10/26/14 Pct Recovery = 116% Analysis Date = 10/26/14 Pct Recovery = 116% Analysis Date = 10/21/14 Pct Recovery = 116% Analysis Date = 10/21/14 Pct Recovery = 116% Analysis Date = 10/16/14 Pct Recovery = 116% Analysis Date = 10/16/14 Pct Recovery = 116% Analysis Date = 10/12/14 Pct Recovery = 116% Analysis Date = 10/12/14 Pct Recovery = 116% Analysis Date = 10/07/14 Pct Recovery = 116% Analysis Date = 10/07/14 Pct Recovery = 116% Analysis Date = 10/02/14 Pct Recovery = 116% Analysis Date = 10/02/14 Pct Recovery = 116% Analysis Date = 09/27/14 Pct Recovery = 116% Analysis Date = 09/27/14 Pct Recovery = 116% Analysis Date = 09/23/14 Pct Recovery = 116% Analysis Date = 09/23/14 Pct Recovery = 116% Analysis Date = 09/18/14 Pct Recovery = 116% Analysis Date = 09/18/14 Pct Recovery = 116% Analysis Date = 09/13/14 Pct Recovery = 116% Analysis Date = 09/13/14 Pct Recovery = 116% Analysis Date = 09/08/14 Pct Recovery = 116% Analysis Date = 09/08/14 Pct Recovery = 116% Analysis Date = 09/04/14 Pct Recovery = 116% Analysis Date = 09/04/14 Pct Recovery = 116% Analysis Date = 08/30/14 Pct Recovery = 116% Analysis Date = 08/30/14 Pct Recovery = 116% Analysis Date = 08/25/14 Pct Recovery = 116% Analysis Date = 08/25/14 Pct Recovery = 116% Analysis Date = 08/20/14 Pct Recovery = 116% Analysis Date = 08/20/14 Pct Recovery = 116% Analysis Date = 08/15/14 Pct Recovery = 116% Analysis Date = 08/15/14 Pct Recovery = 116% Analysis Date = 08/11/14 Pct Recovery = 116% Analysis Date = 08/11/14 Pct Recovery = 116% Analysis Date = 08/06/14 Pct Recovery = 116% Analysis Date = 08/06/14 Pct Recovery = 116% Analysis Date = 08/01/14 Pct Recovery = 116% Analysis Date = 08/01/14 Pct Recovery = 116% Analysis Date = 07/27/14 Pct Recovery = 116% Analysis Date = 07/27/14 Pct Recovery = 116% Analysis Date = 07/23/14 Pct Recovery = 116% Analysis Date = 07/23/14 Pct Recovery = 116% Analysis Date = 07/18/14 Pct Recovery = 116% Analysis Date = 07/18/14 Pct Recovery = 116% Analysis Date = 07/13/14 Pct Recovery = 116% Analysis Date = 07/13/14 Pct Recovery = 116% Analysis Date = 07/08/14 Pct Recovery = 116% Analysis Date = 07/08/14 Pct Recovery = 116% Analysis Date = 07/04/14 Pct Recovery = 116% Analysis Date = 07/04/14 Pct Recovery = 116% Analysis Date = 06/29/14 Pct Recovery = 116% Analysis Date = 06/29/14 Pct Recovery = 116% Analysis Date = 06/24/14 Pct Recovery = 116% Analysis Date = 06/24/14 Pct Recovery = 116% Analysis Date = 06/19/14 Pct Recovery = 116% Analysis Date = 06/19/14 Pct Recovery = 116% Analysis Date = 06/14/14 Pct Recovery = 116% Analysis Date = 06/14/14 Pct Recovery = 116% Analysis Date = 06/10/14 Pct Recovery = 116% Analysis Date = 06/10/14 Pct Recovery = 116% Analysis Date = 06/05/14 Pct Recovery = 116% Analysis Date = 06/05/14 Pct Recovery = 116% Analysis Date = 05/31/14 Pct Recovery = 116% Analysis Date = 05/31/14 Pct Recovery = 116% Analysis Date = 05/26/14 Pct Recovery = 116% Analysis Date = 05/26/14 Pct Recovery = 116% Analysis Date = 05/22/14 Pct Recovery = 116% Analysis Date = 05/22/14 Pct Recovery = 116% Analysis Date = 05/17/14 Pct Recovery = 116% Analysis Date = 05/17/14 Pct Recovery = 116% Analysis Date = 05/12/14 Pct Recovery = 116% Analysis Date = 05/12/14 Pct Recovery = 116% Analysis Date = 05/07/14 Pct Recovery = 116% Analysis Date = 05/07/14 Pct Recovery = 116% Analysis Date = 05/03/14 Pct Recovery = 116% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
1,1-DIFLUOROETHANE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 43 101% 23% 105% 21%
Total 43 101% 23% 105% 21%

Sample Statistics
1,1-DIFLUOROETHANE

Characteristic N % % Basis
Plotted 43 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 43 .  
False Negatives 0 0% 0 out of 43
Not Spiked 30 .  
False Positives 0 0% 0 out of 30

BQS OBSP Determination:
1,2,3,4-TETRAHYDRONAPTHALENE
METHOD: 4440 , TESTIDCODE: 77323GCM66
Open Data Set

Analysis Date = 07/13/15 SpikeMix = Crescent 04EE008: 25 µl & NSI 050515AVOC: 25 µl Pct Recovery = 69% Analysis Date = 12/16/16 SpikeMix = NSI 041816AVOC: 40 µl & ChemService 5082900: 40 µl Pct Recovery = 84% Analysis Date = 08/04/16 SpikeMix = Crescent 03FF058: 40 µl & Supelco LC20141V: 40 µl Pct Recovery = 77% Analysis Date = 07/20/16 SpikeMix = Supelco LC20141V: 40 µl & Accu 216041125: 40 µl Pct Recovery = 100% Analysis Date = 10/17/15 SpikeMix = Crescent 04EE008: 15 µl & NSI 050515AVOC: 15 µl Pct Recovery = 81% Analysis Date = 08/15/15 SpikeMix = Supelco LC13545: 25 µl & Crescent 04EE008: 25 µl Pct Recovery = 85% Analysis Date = 08/26/16 SpikeMix = NSI 041816AVOC: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 73% Analysis Date = 08/12/16 SpikeMix = ChemService 5082900: 25 µl & Phenova B20160319: 25 µl Pct Recovery = 74% Analysis Date = 06/30/16 SpikeMix = Crescent 03FF058: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 75% Analysis Date = 11/21/16 SpikeMix = Crescent 03FF058: 25 µl & Supelco LC20141V: 25 µl Pct Recovery = 87% Analysis Date = 09/08/16 SpikeMix = Supelco LC20141V: 25 µl & Accu 216041125: 25 µl Pct Recovery = 81% Analysis Date = 04/09/15 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 76% Analysis Date = 08/19/14 SpikeMix = Spex Organics C1140417015: 20 µl & Accu 214031115: 20 µl Pct Recovery = 90% Analysis Date = 07/01/14 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 80% Analysis Date = 05/01/14 SpikeMix = Accu 214031115: 20 µl & NSI 032614: 20 µl Pct Recovery = 75% Analysis Date = 03/19/15 SpikeMix = Spex Organics C1140417015: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 79% Analysis Date = 12/17/14 SpikeMix = Supelco LC06438: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 74% Analysis Date = 11/14/14 SpikeMix = Crescent 03DD004: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 78% Analysis Date = 06/10/14 SpikeMix = Crescent 03DD004: 20 µl & NSI 032614: 20 µl Pct Recovery = 72% Analysis Date = 09/29/15 SpikeMix = Accu 215041380: 25 µl & ERA 0406-15-03: 25 µl Pct Recovery = 91% Analysis Date = 06/16/15 SpikeMix = ERA 0406-15-03: 25 µl & Supelco LC13545: 25 µl Pct Recovery = 74% Analysis Date = 01/27/16 SpikeMix = Crescent 04EE008: 10 µl & NSI 050515AVOC: 10 µl Pct Recovery = 84% Analysis Date = 07/31/15 SpikeMix = Crescent 04EE008: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 70% Analysis Date = 12/18/15 SpikeMix = Supelco LC13545: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 85% Analysis Date = 05/09/15 SpikeMix = Spex Organics EN150428007: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 75% Analysis Date = 11/29/16 SpikeMix = ChemService 5082900: 15 µl & Phenova B20160319: 15 µl Pct Recovery = 78% Analysis Date = 09/28/16 SpikeMix = Crescent 03FF058: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 71% Analysis Date = 06/30/16 SpikeMix = ChemService 5082900: 15 µl & Accu 216041125: 15 µl Pct Recovery = 76% Analysis Date = 06/10/16 SpikeMix = NSI 041816AVOC: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 82% Analysis Date = 10/13/16 SpikeMix = NSI 041816AVOC: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 78% Analysis Date = 05/27/16 SpikeMix = Phenova B20160319: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 81% Analysis Date = 11/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 111% Analysis Date = 06/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Accu 215041380: 15 µl Pct Recovery = 82% Analysis Date = 04/26/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 84% Analysis Date = 03/04/16 SpikeMix = Accu 215041380: 15 µl & ERA 0406-15-03: 15 µl Pct Recovery = 75% Analysis Date = 02/05/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 81% Analysis Date = 10/16/15 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 85% Analysis Date = 01/13/15 SpikeMix = Accu 214031115: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 87% Analysis Date = 09/09/14 SpikeMix = Accu 214031115: 10 µl & NSI 032614: 10 µl Pct Recovery = 117% Analysis Date = 07/23/14 SpikeMix = Spex Organics C1140417015: 10 µl & Accu 214031115: 10 µl Pct Recovery = 88% Analysis Date = 06/18/14 SpikeMix = Supelco LC06438: 10 µl & Accu 214031115: 10 µl Pct Recovery = 79% Analysis Date = 11/06/14 SpikeMix = Spex Organics C1140417015: 10 µl & Crescent 03DD004: 10 µl Pct Recovery = 91% Analysis Date = 10/04/14 SpikeMix = Crescent 03DD004: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 79% Analysis Date = 07/29/14 SpikeMix = Crescent 03DD004: 10 µl & NSI 032614: 10 µl Pct Recovery = 82% Analysis Date = 05/03/14 SpikeMix = Crescent 03DD004: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 86% Analysis Date = 05/13/16 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 82% Analysis Date = 05/09/15 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 77% Analysis Date = 03/17/16 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 67% Analysis Date = 12/10/15 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 90% Analysis Date = 09/03/15 SpikeMix = NSI 050515AVOC: 10 µl & Spex Organics EN150428007: 10 µl Pct Recovery = 86% Analysis Date = 11/20/15 SpikeMix = Accu 215041380: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 91% Analysis Date = 06/27/15 SpikeMix = ERA 0406-15-03: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 106% Analysis Date = 12/15/16 Pct Recovery = 79% Analysis Date = 12/11/16 Pct Recovery = 79% Analysis Date = 12/11/16 Pct Recovery = 79% Analysis Date = 12/06/16 Pct Recovery = 79% Analysis Date = 12/06/16 Pct Recovery = 79% Analysis Date = 12/01/16 Pct Recovery = 79% Analysis Date = 12/01/16 Pct Recovery = 79% Analysis Date = 11/26/16 Pct Recovery = 79% Analysis Date = 11/26/16 Pct Recovery = 79% Analysis Date = 11/21/16 Pct Recovery = 79% Analysis Date = 11/21/16 Pct Recovery = 79% Analysis Date = 11/17/16 Pct Recovery = 79% Analysis Date = 11/17/16 Pct Recovery = 79% Analysis Date = 11/12/16 Pct Recovery = 79% Analysis Date = 11/12/16 Pct Recovery = 79% Analysis Date = 11/07/16 Pct Recovery = 79% Analysis Date = 11/07/16 Pct Recovery = 79% Analysis Date = 11/02/16 Pct Recovery = 79% Analysis Date = 11/02/16 Pct Recovery = 79% Analysis Date = 10/28/16 Pct Recovery = 79% Analysis Date = 10/28/16 Pct Recovery = 79% Analysis Date = 10/24/16 Pct Recovery = 79% Analysis Date = 10/24/16 Pct Recovery = 79% Analysis Date = 10/19/16 Pct Recovery = 79% Analysis Date = 10/19/16 Pct Recovery = 79% Analysis Date = 10/14/16 Pct Recovery = 79% Analysis Date = 10/14/16 Pct Recovery = 79% Analysis Date = 10/09/16 Pct Recovery = 79% Analysis Date = 10/09/16 Pct Recovery = 79% Analysis Date = 10/04/16 Pct Recovery = 79% Analysis Date = 10/04/16 Pct Recovery = 79% Analysis Date = 09/30/16 Pct Recovery = 79% Analysis Date = 09/30/16 Pct Recovery = 79% Analysis Date = 09/25/16 Pct Recovery = 79% Analysis Date = 09/25/16 Pct Recovery = 79% Analysis Date = 09/20/16 Pct Recovery = 79% Analysis Date = 09/20/16 Pct Recovery = 79% Analysis Date = 09/15/16 Pct Recovery = 80% Analysis Date = 09/15/16 Pct Recovery = 80% Analysis Date = 09/10/16 Pct Recovery = 80% Analysis Date = 09/10/16 Pct Recovery = 80% Analysis Date = 09/06/16 Pct Recovery = 80% Analysis Date = 09/06/16 Pct Recovery = 80% Analysis Date = 09/01/16 Pct Recovery = 80% Analysis Date = 09/01/16 Pct Recovery = 80% Analysis Date = 08/27/16 Pct Recovery = 80% Analysis Date = 08/27/16 Pct Recovery = 80% Analysis Date = 08/22/16 Pct Recovery = 80% Analysis Date = 08/22/16 Pct Recovery = 80% Analysis Date = 08/17/16 Pct Recovery = 80% Analysis Date = 08/17/16 Pct Recovery = 80% Analysis Date = 08/13/16 Pct Recovery = 80% Analysis Date = 08/13/16 Pct Recovery = 80% Analysis Date = 08/08/16 Pct Recovery = 80% Analysis Date = 08/08/16 Pct Recovery = 80% Analysis Date = 08/03/16 Pct Recovery = 80% Analysis Date = 08/03/16 Pct Recovery = 80% Analysis Date = 07/29/16 Pct Recovery = 80% Analysis Date = 07/29/16 Pct Recovery = 80% Analysis Date = 07/24/16 Pct Recovery = 80% Analysis Date = 07/24/16 Pct Recovery = 80% Analysis Date = 07/20/16 Pct Recovery = 80% Analysis Date = 07/20/16 Pct Recovery = 80% Analysis Date = 07/15/16 Pct Recovery = 80% Analysis Date = 07/15/16 Pct Recovery = 80% Analysis Date = 07/10/16 Pct Recovery = 80% Analysis Date = 07/10/16 Pct Recovery = 80% Analysis Date = 07/05/16 Pct Recovery = 80% Analysis Date = 07/05/16 Pct Recovery = 80% Analysis Date = 06/30/16 Pct Recovery = 80% Analysis Date = 06/30/16 Pct Recovery = 80% Analysis Date = 06/26/16 Pct Recovery = 80% Analysis Date = 06/26/16 Pct Recovery = 80% Analysis Date = 06/21/16 Pct Recovery = 81% Analysis Date = 06/21/16 Pct Recovery = 81% Analysis Date = 06/16/16 Pct Recovery = 81% Analysis Date = 06/16/16 Pct Recovery = 81% Analysis Date = 06/11/16 Pct Recovery = 81% Analysis Date = 06/11/16 Pct Recovery = 81% Analysis Date = 06/06/16 Pct Recovery = 81% Analysis Date = 06/06/16 Pct Recovery = 81% Analysis Date = 06/02/16 Pct Recovery = 81% Analysis Date = 06/02/16 Pct Recovery = 81% Analysis Date = 05/28/16 Pct Recovery = 81% Analysis Date = 05/28/16 Pct Recovery = 81% Analysis Date = 05/23/16 Pct Recovery = 81% Analysis Date = 05/23/16 Pct Recovery = 81% Analysis Date = 05/18/16 Pct Recovery = 81% Analysis Date = 05/18/16 Pct Recovery = 81% Analysis Date = 05/13/16 Pct Recovery = 81% Analysis Date = 05/13/16 Pct Recovery = 81% Analysis Date = 05/09/16 Pct Recovery = 81% Analysis Date = 05/09/16 Pct Recovery = 81% Analysis Date = 05/04/16 Pct Recovery = 81% Analysis Date = 05/04/16 Pct Recovery = 81% Analysis Date = 04/29/16 Pct Recovery = 82% Analysis Date = 04/29/16 Pct Recovery = 82% Analysis Date = 04/24/16 Pct Recovery = 82% Analysis Date = 04/24/16 Pct Recovery = 82% Analysis Date = 04/19/16 Pct Recovery = 82% Analysis Date = 04/19/16 Pct Recovery = 82% Analysis Date = 04/15/16 Pct Recovery = 82% Analysis Date = 04/15/16 Pct Recovery = 82% Analysis Date = 04/10/16 Pct Recovery = 82% Analysis Date = 04/10/16 Pct Recovery = 82% Analysis Date = 04/05/16 Pct Recovery = 82% Analysis Date = 04/05/16 Pct Recovery = 82% Analysis Date = 03/31/16 Pct Recovery = 82% Analysis Date = 03/31/16 Pct Recovery = 82% Analysis Date = 03/26/16 Pct Recovery = 82% Analysis Date = 03/26/16 Pct Recovery = 82% Analysis Date = 03/22/16 Pct Recovery = 82% Analysis Date = 03/22/16 Pct Recovery = 82% Analysis Date = 03/17/16 Pct Recovery = 83% Analysis Date = 03/17/16 Pct Recovery = 83% Analysis Date = 03/12/16 Pct Recovery = 83% Analysis Date = 03/12/16 Pct Recovery = 83% Analysis Date = 03/07/16 Pct Recovery = 83% Analysis Date = 03/07/16 Pct Recovery = 83% Analysis Date = 03/02/16 Pct Recovery = 83% Analysis Date = 03/02/16 Pct Recovery = 83% Analysis Date = 02/27/16 Pct Recovery = 83% Analysis Date = 02/27/16 Pct Recovery = 83% Analysis Date = 02/22/16 Pct Recovery = 83% Analysis Date = 02/22/16 Pct Recovery = 83% Analysis Date = 02/17/16 Pct Recovery = 83% Analysis Date = 02/17/16 Pct Recovery = 83% Analysis Date = 02/12/16 Pct Recovery = 83% Analysis Date = 02/12/16 Pct Recovery = 83% Analysis Date = 02/07/16 Pct Recovery = 83% Analysis Date = 02/07/16 Pct Recovery = 83% Analysis Date = 02/03/16 Pct Recovery = 84% Analysis Date = 02/03/16 Pct Recovery = 84% Analysis Date = 01/29/16 Pct Recovery = 84% Analysis Date = 01/29/16 Pct Recovery = 84% Analysis Date = 01/24/16 Pct Recovery = 84% Analysis Date = 01/24/16 Pct Recovery = 84% Analysis Date = 01/19/16 Pct Recovery = 84% Analysis Date = 01/19/16 Pct Recovery = 84% Analysis Date = 01/14/16 Pct Recovery = 84% Analysis Date = 01/14/16 Pct Recovery = 84% Analysis Date = 01/10/16 Pct Recovery = 84% Analysis Date = 01/10/16 Pct Recovery = 84% Analysis Date = 01/05/16 Pct Recovery = 84% Analysis Date = 01/05/16 Pct Recovery = 84% Analysis Date = 12/31/15 Pct Recovery = 84% Analysis Date = 12/31/15 Pct Recovery = 84% Analysis Date = 12/26/15 Pct Recovery = 84% Analysis Date = 12/26/15 Pct Recovery = 84% Analysis Date = 12/21/15 Pct Recovery = 84% Analysis Date = 12/21/15 Pct Recovery = 84% Analysis Date = 12/17/15 Pct Recovery = 84% Analysis Date = 12/17/15 Pct Recovery = 84% Analysis Date = 12/12/15 Pct Recovery = 84% Analysis Date = 12/12/15 Pct Recovery = 84% Analysis Date = 12/07/15 Pct Recovery = 84% Analysis Date = 12/07/15 Pct Recovery = 84% Analysis Date = 12/02/15 Pct Recovery = 84% Analysis Date = 12/02/15 Pct Recovery = 84% Analysis Date = 11/27/15 Pct Recovery = 84% Analysis Date = 11/27/15 Pct Recovery = 84% Analysis Date = 11/23/15 Pct Recovery = 84% Analysis Date = 11/23/15 Pct Recovery = 84% Analysis Date = 11/18/15 Pct Recovery = 84% Analysis Date = 11/18/15 Pct Recovery = 84% Analysis Date = 11/13/15 Pct Recovery = 84% Analysis Date = 11/13/15 Pct Recovery = 84% Analysis Date = 11/08/15 Pct Recovery = 84% Analysis Date = 11/08/15 Pct Recovery = 84% Analysis Date = 11/03/15 Pct Recovery = 84% Analysis Date = 11/03/15 Pct Recovery = 84% Analysis Date = 10/30/15 Pct Recovery = 84% Analysis Date = 10/30/15 Pct Recovery = 84% Analysis Date = 10/25/15 Pct Recovery = 84% Analysis Date = 10/25/15 Pct Recovery = 84% Analysis Date = 10/20/15 Pct Recovery = 84% Analysis Date = 10/20/15 Pct Recovery = 84% Analysis Date = 10/15/15 Pct Recovery = 84% Analysis Date = 10/15/15 Pct Recovery = 84% Analysis Date = 10/10/15 Pct Recovery = 84% Analysis Date = 10/10/15 Pct Recovery = 84% Analysis Date = 10/06/15 Pct Recovery = 84% Analysis Date = 10/06/15 Pct Recovery = 84% Analysis Date = 10/01/15 Pct Recovery = 84% Analysis Date = 10/01/15 Pct Recovery = 84% Analysis Date = 09/26/15 Pct Recovery = 84% Analysis Date = 09/26/15 Pct Recovery = 84% Analysis Date = 09/21/15 Pct Recovery = 84% Analysis Date = 09/21/15 Pct Recovery = 84% Analysis Date = 09/16/15 Pct Recovery = 84% Analysis Date = 09/16/15 Pct Recovery = 84% Analysis Date = 09/12/15 Pct Recovery = 83% Analysis Date = 09/12/15 Pct Recovery = 83% Analysis Date = 09/07/15 Pct Recovery = 83% Analysis Date = 09/07/15 Pct Recovery = 83% Analysis Date = 09/02/15 Pct Recovery = 83% Analysis Date = 09/02/15 Pct Recovery = 83% Analysis Date = 08/28/15 Pct Recovery = 83% Analysis Date = 08/28/15 Pct Recovery = 83% Analysis Date = 08/23/15 Pct Recovery = 83% Analysis Date = 08/23/15 Pct Recovery = 83% Analysis Date = 08/19/15 Pct Recovery = 83% Analysis Date = 08/19/15 Pct Recovery = 83% Analysis Date = 08/14/15 Pct Recovery = 83% Analysis Date = 08/14/15 Pct Recovery = 83% Analysis Date = 08/09/15 Pct Recovery = 83% Analysis Date = 08/09/15 Pct Recovery = 83% Analysis Date = 08/04/15 Pct Recovery = 83% Analysis Date = 08/04/15 Pct Recovery = 83% Analysis Date = 07/30/15 Pct Recovery = 83% Analysis Date = 07/30/15 Pct Recovery = 83% Analysis Date = 07/26/15 Pct Recovery = 83% Analysis Date = 07/26/15 Pct Recovery = 83% Analysis Date = 07/21/15 Pct Recovery = 83% Analysis Date = 07/21/15 Pct Recovery = 83% Analysis Date = 07/16/15 Pct Recovery = 83% Analysis Date = 07/16/15 Pct Recovery = 83% Analysis Date = 07/11/15 Pct Recovery = 83% Analysis Date = 07/11/15 Pct Recovery = 83% Analysis Date = 07/06/15 Pct Recovery = 83% Analysis Date = 07/06/15 Pct Recovery = 83% Analysis Date = 07/02/15 Pct Recovery = 83% Analysis Date = 07/02/15 Pct Recovery = 83% Analysis Date = 06/27/15 Pct Recovery = 83% Analysis Date = 06/27/15 Pct Recovery = 83% Analysis Date = 06/22/15 Pct Recovery = 83% Analysis Date = 06/22/15 Pct Recovery = 83% Analysis Date = 06/17/15 Pct Recovery = 83% Analysis Date = 06/17/15 Pct Recovery = 83% Analysis Date = 06/12/15 Pct Recovery = 82% Analysis Date = 06/12/15 Pct Recovery = 82% Analysis Date = 06/08/15 Pct Recovery = 82% Analysis Date = 06/08/15 Pct Recovery = 82% Analysis Date = 06/03/15 Pct Recovery = 82% Analysis Date = 06/03/15 Pct Recovery = 82% Analysis Date = 05/29/15 Pct Recovery = 82% Analysis Date = 05/29/15 Pct Recovery = 82% Analysis Date = 05/24/15 Pct Recovery = 82% Analysis Date = 05/24/15 Pct Recovery = 82% Analysis Date = 05/19/15 Pct Recovery = 82% Analysis Date = 05/19/15 Pct Recovery = 82% Analysis Date = 05/15/15 Pct Recovery = 82% Analysis Date = 05/15/15 Pct Recovery = 82% Analysis Date = 05/10/15 Pct Recovery = 82% Analysis Date = 05/10/15 Pct Recovery = 82% Analysis Date = 05/05/15 Pct Recovery = 82% Analysis Date = 05/05/15 Pct Recovery = 82% Analysis Date = 04/30/15 Pct Recovery = 82% Analysis Date = 04/30/15 Pct Recovery = 82% Analysis Date = 04/25/15 Pct Recovery = 82% Analysis Date = 04/25/15 Pct Recovery = 82% Analysis Date = 04/21/15 Pct Recovery = 82% Analysis Date = 04/21/15 Pct Recovery = 82% Analysis Date = 04/16/15 Pct Recovery = 82% Analysis Date = 04/16/15 Pct Recovery = 82% Analysis Date = 04/11/15 Pct Recovery = 82% Analysis Date = 04/11/15 Pct Recovery = 82% Analysis Date = 04/06/15 Pct Recovery = 82% Analysis Date = 04/06/15 Pct Recovery = 82% Analysis Date = 04/01/15 Pct Recovery = 82% Analysis Date = 04/01/15 Pct Recovery = 82% Analysis Date = 03/28/15 Pct Recovery = 82% Analysis Date = 03/28/15 Pct Recovery = 82% Analysis Date = 03/23/15 Pct Recovery = 82% Analysis Date = 03/23/15 Pct Recovery = 82% Analysis Date = 03/18/15 Pct Recovery = 82% Analysis Date = 03/18/15 Pct Recovery = 82% Analysis Date = 03/13/15 Pct Recovery = 83% Analysis Date = 03/13/15 Pct Recovery = 83% Analysis Date = 03/08/15 Pct Recovery = 83% Analysis Date = 03/08/15 Pct Recovery = 83% Analysis Date = 03/04/15 Pct Recovery = 83% Analysis Date = 03/04/15 Pct Recovery = 83% Analysis Date = 02/27/15 Pct Recovery = 83% Analysis Date = 02/27/15 Pct Recovery = 83% Analysis Date = 02/22/15 Pct Recovery = 83% Analysis Date = 02/22/15 Pct Recovery = 83% Analysis Date = 02/17/15 Pct Recovery = 83% Analysis Date = 02/17/15 Pct Recovery = 83% Analysis Date = 02/12/15 Pct Recovery = 83% Analysis Date = 02/12/15 Pct Recovery = 83% Analysis Date = 02/08/15 Pct Recovery = 83% Analysis Date = 02/08/15 Pct Recovery = 83% Analysis Date = 02/03/15 Pct Recovery = 83% Analysis Date = 02/03/15 Pct Recovery = 83% Analysis Date = 01/29/15 Pct Recovery = 83% Analysis Date = 01/29/15 Pct Recovery = 83% Analysis Date = 01/24/15 Pct Recovery = 83% Analysis Date = 01/24/15 Pct Recovery = 83% Analysis Date = 01/19/15 Pct Recovery = 83% Analysis Date = 01/19/15 Pct Recovery = 83% Analysis Date = 01/15/15 Pct Recovery = 83% Analysis Date = 01/15/15 Pct Recovery = 83% Analysis Date = 01/10/15 Pct Recovery = 83% Analysis Date = 01/10/15 Pct Recovery = 83% Analysis Date = 01/05/15 Pct Recovery = 83% Analysis Date = 01/05/15 Pct Recovery = 83% Analysis Date = 12/31/14 Pct Recovery = 83% Analysis Date = 12/31/14 Pct Recovery = 83% Analysis Date = 12/26/14 Pct Recovery = 83% Analysis Date = 12/26/14 Pct Recovery = 83% Analysis Date = 12/22/14 Pct Recovery = 83% Analysis Date = 12/22/14 Pct Recovery = 83% Analysis Date = 12/17/14 Pct Recovery = 83% Analysis Date = 12/17/14 Pct Recovery = 83% Analysis Date = 12/12/14 Pct Recovery = 83% Analysis Date = 12/12/14 Pct Recovery = 83% Analysis Date = 12/07/14 Pct Recovery = 83% Analysis Date = 12/07/14 Pct Recovery = 83% Analysis Date = 12/02/14 Pct Recovery = 83% Analysis Date = 12/02/14 Pct Recovery = 83% Analysis Date = 11/28/14 Pct Recovery = 83% Analysis Date = 11/28/14 Pct Recovery = 83% Analysis Date = 11/23/14 Pct Recovery = 83% Analysis Date = 11/23/14 Pct Recovery = 83% Analysis Date = 11/18/14 Pct Recovery = 83% Analysis Date = 11/18/14 Pct Recovery = 83% Analysis Date = 11/13/14 Pct Recovery = 83% Analysis Date = 11/13/14 Pct Recovery = 83% Analysis Date = 11/08/14 Pct Recovery = 83% Analysis Date = 11/08/14 Pct Recovery = 83% Analysis Date = 11/04/14 Pct Recovery = 83% Analysis Date = 11/04/14 Pct Recovery = 83% Analysis Date = 10/30/14 Pct Recovery = 83% Analysis Date = 10/30/14 Pct Recovery = 83% Analysis Date = 10/25/14 Pct Recovery = 83% Analysis Date = 10/25/14 Pct Recovery = 83% Analysis Date = 10/20/14 Pct Recovery = 83% Analysis Date = 10/20/14 Pct Recovery = 83% Analysis Date = 10/15/14 Pct Recovery = 83% Analysis Date = 10/15/14 Pct Recovery = 83% Analysis Date = 10/11/14 Pct Recovery = 83% Analysis Date = 10/11/14 Pct Recovery = 83% Analysis Date = 10/06/14 Pct Recovery = 83% Analysis Date = 10/06/14 Pct Recovery = 83% Analysis Date = 10/01/14 Pct Recovery = 83% Analysis Date = 10/01/14 Pct Recovery = 83% Analysis Date = 09/26/14 Pct Recovery = 83% Analysis Date = 09/26/14 Pct Recovery = 83% Analysis Date = 09/21/14 Pct Recovery = 83% Analysis Date = 09/21/14 Pct Recovery = 83% Analysis Date = 09/17/14 Pct Recovery = 83% Analysis Date = 09/17/14 Pct Recovery = 83% Analysis Date = 09/12/14 Pct Recovery = 83% Analysis Date = 09/12/14 Pct Recovery = 83% Analysis Date = 09/07/14 Pct Recovery = 83% Analysis Date = 09/07/14 Pct Recovery = 83% Analysis Date = 09/02/14 Pct Recovery = 83% Analysis Date = 09/02/14 Pct Recovery = 83% Analysis Date = 08/28/14 Pct Recovery = 83% Analysis Date = 08/28/14 Pct Recovery = 83% Analysis Date = 08/24/14 Pct Recovery = 83% Analysis Date = 08/24/14 Pct Recovery = 83% Analysis Date = 08/19/14 Pct Recovery = 83% Analysis Date = 08/19/14 Pct Recovery = 83% Analysis Date = 08/14/14 Pct Recovery = 84% Analysis Date = 08/14/14 Pct Recovery = 84% Analysis Date = 08/09/14 Pct Recovery = 84% Analysis Date = 08/09/14 Pct Recovery = 84% Analysis Date = 08/04/14 Pct Recovery = 84% Analysis Date = 08/04/14 Pct Recovery = 84% Analysis Date = 07/31/14 Pct Recovery = 84% Analysis Date = 07/31/14 Pct Recovery = 84% Analysis Date = 07/26/14 Pct Recovery = 84% Analysis Date = 07/26/14 Pct Recovery = 84% Analysis Date = 07/21/14 Pct Recovery = 84% Analysis Date = 07/21/14 Pct Recovery = 84% Analysis Date = 07/16/14 Pct Recovery = 84% Analysis Date = 07/16/14 Pct Recovery = 84% Analysis Date = 07/11/14 Pct Recovery = 84% Analysis Date = 07/11/14 Pct Recovery = 84% Analysis Date = 07/07/14 Pct Recovery = 84% Analysis Date = 07/07/14 Pct Recovery = 84% Analysis Date = 07/02/14 Pct Recovery = 84% Analysis Date = 07/02/14 Pct Recovery = 84% Analysis Date = 06/27/14 Pct Recovery = 84% Analysis Date = 06/27/14 Pct Recovery = 84% Analysis Date = 06/22/14 Pct Recovery = 84% Analysis Date = 06/22/14 Pct Recovery = 84% Analysis Date = 06/17/14 Pct Recovery = 84% Analysis Date = 06/17/14 Pct Recovery = 84% Analysis Date = 06/13/14 Pct Recovery = 84% Analysis Date = 06/13/14 Pct Recovery = 84% Analysis Date = 06/08/14 Pct Recovery = 84% Analysis Date = 06/08/14 Pct Recovery = 84% Analysis Date = 06/03/14 Pct Recovery = 84% Analysis Date = 06/03/14 Pct Recovery = 84% Analysis Date = 05/29/14 Pct Recovery = 84% Analysis Date = 05/29/14 Pct Recovery = 84% Analysis Date = 05/24/14 Pct Recovery = 84% Analysis Date = 05/24/14 Pct Recovery = 84% Analysis Date = 05/20/14 Pct Recovery = 84% Analysis Date = 05/20/14 Pct Recovery = 84% Analysis Date = 05/15/14 Pct Recovery = 84% Analysis Date = 05/15/14 Pct Recovery = 84% Analysis Date = 05/10/14 Pct Recovery = 84% Analysis Date = 05/10/14 Pct Recovery = 84% Analysis Date = 05/05/14 Pct Recovery = 84% Analysis Date = 05/05/14 Pct Recovery = 84% Analysis Date = 05/01/14 Pct Recovery = 84% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
1,2,3,4-TETRAHYDRONAPTHALENE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 52 82% 10% 81% 8%
Total 52 82% 10% 81% 8%

Sample Statistics
1,2,3,4-TETRAHYDRONAPTHALENE

Characteristic N % % Basis
Plotted 52 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 52 .  
False Negatives 0 0% 0 out of 52
Not Spiked 21 .  
False Positives 0 0% 0 out of 21

BQS OBSP Determination:
1,2,3,4-TETRAMETHYLBENZENE
METHOD: 4440 , TESTIDCODE: 49999GCM66
Open Data Set

Analysis Date = 12/12/16 SpikeMix = Accu 216041125: 40 µl & Crescent 03FF058: 40 µl Pct Recovery = 104% Analysis Date = 07/20/16 SpikeMix = Supelco LC20141V: 40 µl & Accu 216041125: 40 µl Pct Recovery = 88% Analysis Date = 07/14/16 SpikeMix = Accu 216041125: 40 µl & NSI 041816AVOC: 40 µl Pct Recovery = 78% Analysis Date = 09/08/16 SpikeMix = Supelco LC20141V: 25 µl & Accu 216041125: 25 µl Pct Recovery = 64% Analysis Date = 05/24/16 SpikeMix = Accu 216041125: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 90% Analysis Date = 04/09/15 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 76% Analysis Date = 08/19/14 SpikeMix = Spex Organics C1140417015: 20 µl & Accu 214031115: 20 µl Pct Recovery = 105% Analysis Date = 07/01/14 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 82% Analysis Date = 05/01/14 SpikeMix = Accu 214031115: 20 µl & NSI 032614: 20 µl Pct Recovery = 81% Analysis Date = 03/19/15 SpikeMix = Spex Organics C1140417015: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 78% Analysis Date = 12/17/14 SpikeMix = Supelco LC06438: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 87% Analysis Date = 11/14/14 SpikeMix = Crescent 03DD004: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 86% Analysis Date = 06/10/14 SpikeMix = Crescent 03DD004: 20 µl & NSI 032614: 20 µl Pct Recovery = 74% Analysis Date = 09/29/15 SpikeMix = Accu 215041380: 25 µl & ERA 0406-15-03: 25 µl Pct Recovery = 86% Analysis Date = 10/13/16 SpikeMix = Accu 216041125: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 86% Analysis Date = 08/20/16 SpikeMix = Accu 216041125: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 99% Analysis Date = 06/30/16 SpikeMix = ChemService 5082900: 15 µl & Accu 216041125: 15 µl Pct Recovery = 54% Analysis Date = 04/02/16 SpikeMix = Supelco LC13545: 15 µl & Accu 215041380: 15 µl Pct Recovery = 82% Analysis Date = 03/04/16 SpikeMix = Accu 215041380: 15 µl & ERA 0406-15-03: 15 µl Pct Recovery = 72% Analysis Date = 06/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Accu 215041380: 15 µl Pct Recovery = 78% Analysis Date = 01/13/15 SpikeMix = Accu 214031115: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 102% Analysis Date = 09/09/14 SpikeMix = Accu 214031115: 10 µl & NSI 032614: 10 µl Pct Recovery = 143% Analysis Date = 07/23/14 SpikeMix = Spex Organics C1140417015: 10 µl & Accu 214031115: 10 µl Pct Recovery = 97% Analysis Date = 06/18/14 SpikeMix = Supelco LC06438: 10 µl & Accu 214031115: 10 µl Pct Recovery = 76% Analysis Date = 11/06/14 SpikeMix = Spex Organics C1140417015: 10 µl & Crescent 03DD004: 10 µl Pct Recovery = 97% Analysis Date = 10/04/14 SpikeMix = Crescent 03DD004: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 92% Analysis Date = 07/29/14 SpikeMix = Crescent 03DD004: 10 µl & NSI 032614: 10 µl Pct Recovery = 128% Analysis Date = 05/03/14 SpikeMix = Crescent 03DD004: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 105% Analysis Date = 02/18/16 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 81% Analysis Date = 11/20/15 SpikeMix = Accu 215041380: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 103% Analysis Date = 11/12/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 90% Analysis Date = 05/21/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 110% Analysis Date = 12/11/16 Pct Recovery = 84% Analysis Date = 12/07/16 Pct Recovery = 84% Analysis Date = 12/07/16 Pct Recovery = 84% Analysis Date = 12/02/16 Pct Recovery = 84% Analysis Date = 12/02/16 Pct Recovery = 84% Analysis Date = 11/27/16 Pct Recovery = 83% Analysis Date = 11/27/16 Pct Recovery = 83% Analysis Date = 11/22/16 Pct Recovery = 83% Analysis Date = 11/22/16 Pct Recovery = 83% Analysis Date = 11/18/16 Pct Recovery = 83% Analysis Date = 11/18/16 Pct Recovery = 83% Analysis Date = 11/13/16 Pct Recovery = 83% Analysis Date = 11/13/16 Pct Recovery = 83% Analysis Date = 11/08/16 Pct Recovery = 83% Analysis Date = 11/08/16 Pct Recovery = 83% Analysis Date = 11/03/16 Pct Recovery = 83% Analysis Date = 11/03/16 Pct Recovery = 83% Analysis Date = 10/29/16 Pct Recovery = 83% Analysis Date = 10/29/16 Pct Recovery = 83% Analysis Date = 10/25/16 Pct Recovery = 83% Analysis Date = 10/25/16 Pct Recovery = 83% Analysis Date = 10/20/16 Pct Recovery = 83% Analysis Date = 10/20/16 Pct Recovery = 83% Analysis Date = 10/15/16 Pct Recovery = 83% Analysis Date = 10/15/16 Pct Recovery = 83% Analysis Date = 10/10/16 Pct Recovery = 83% Analysis Date = 10/10/16 Pct Recovery = 83% Analysis Date = 10/06/16 Pct Recovery = 83% Analysis Date = 10/06/16 Pct Recovery = 83% Analysis Date = 10/01/16 Pct Recovery = 83% Analysis Date = 10/01/16 Pct Recovery = 83% Analysis Date = 09/26/16 Pct Recovery = 83% Analysis Date = 09/26/16 Pct Recovery = 83% Analysis Date = 09/21/16 Pct Recovery = 83% Analysis Date = 09/21/16 Pct Recovery = 83% Analysis Date = 09/16/16 Pct Recovery = 83% Analysis Date = 09/16/16 Pct Recovery = 83% Analysis Date = 09/12/16 Pct Recovery = 83% Analysis Date = 09/12/16 Pct Recovery = 83% Analysis Date = 09/07/16 Pct Recovery = 83% Analysis Date = 09/07/16 Pct Recovery = 83% Analysis Date = 09/02/16 Pct Recovery = 83% Analysis Date = 09/02/16 Pct Recovery = 83% Analysis Date = 08/28/16 Pct Recovery = 83% Analysis Date = 08/28/16 Pct Recovery = 83% Analysis Date = 08/24/16 Pct Recovery = 83% Analysis Date = 08/24/16 Pct Recovery = 83% Analysis Date = 08/19/16 Pct Recovery = 83% Analysis Date = 08/19/16 Pct Recovery = 83% Analysis Date = 08/14/16 Pct Recovery = 83% Analysis Date = 08/14/16 Pct Recovery = 83% Analysis Date = 08/09/16 Pct Recovery = 83% Analysis Date = 08/09/16 Pct Recovery = 83% Analysis Date = 08/04/16 Pct Recovery = 83% Analysis Date = 08/04/16 Pct Recovery = 83% Analysis Date = 07/31/16 Pct Recovery = 83% Analysis Date = 07/31/16 Pct Recovery = 83% Analysis Date = 07/26/16 Pct Recovery = 83% Analysis Date = 07/26/16 Pct Recovery = 83% Analysis Date = 07/21/16 Pct Recovery = 83% Analysis Date = 07/21/16 Pct Recovery = 83% Analysis Date = 07/16/16 Pct Recovery = 83% Analysis Date = 07/16/16 Pct Recovery = 83% Analysis Date = 07/12/16 Pct Recovery = 83% Analysis Date = 07/12/16 Pct Recovery = 83% Analysis Date = 07/07/16 Pct Recovery = 83% Analysis Date = 07/07/16 Pct Recovery = 83% Analysis Date = 07/02/16 Pct Recovery = 83% Analysis Date = 07/02/16 Pct Recovery = 83% Analysis Date = 06/27/16 Pct Recovery = 83% Analysis Date = 06/27/16 Pct Recovery = 83% Analysis Date = 06/22/16 Pct Recovery = 83% Analysis Date = 06/22/16 Pct Recovery = 83% Analysis Date = 06/18/16 Pct Recovery = 83% Analysis Date = 06/18/16 Pct Recovery = 83% Analysis Date = 06/13/16 Pct Recovery = 83% Analysis Date = 06/13/16 Pct Recovery = 83% Analysis Date = 06/08/16 Pct Recovery = 83% Analysis Date = 06/08/16 Pct Recovery = 83% Analysis Date = 06/03/16 Pct Recovery = 83% Analysis Date = 06/03/16 Pct Recovery = 83% Analysis Date = 05/30/16 Pct Recovery = 83% Analysis Date = 05/30/16 Pct Recovery = 83% Analysis Date = 05/25/16 Pct Recovery = 84% Analysis Date = 05/25/16 Pct Recovery = 84% Analysis Date = 05/20/16 Pct Recovery = 84% Analysis Date = 05/20/16 Pct Recovery = 84% Analysis Date = 05/15/16 Pct Recovery = 84% Analysis Date = 05/15/16 Pct Recovery = 84% Analysis Date = 05/10/16 Pct Recovery = 84% Analysis Date = 05/10/16 Pct Recovery = 84% Analysis Date = 05/06/16 Pct Recovery = 84% Analysis Date = 05/06/16 Pct Recovery = 84% Analysis Date = 05/01/16 Pct Recovery = 84% Analysis Date = 05/01/16 Pct Recovery = 84% Analysis Date = 04/26/16 Pct Recovery = 84% Analysis Date = 04/26/16 Pct Recovery = 84% Analysis Date = 04/21/16 Pct Recovery = 84% Analysis Date = 04/21/16 Pct Recovery = 84% Analysis Date = 04/16/16 Pct Recovery = 84% Analysis Date = 04/16/16 Pct Recovery = 84% Analysis Date = 04/12/16 Pct Recovery = 84% Analysis Date = 04/12/16 Pct Recovery = 84% Analysis Date = 04/07/16 Pct Recovery = 84% Analysis Date = 04/07/16 Pct Recovery = 84% Analysis Date = 04/02/16 Pct Recovery = 84% Analysis Date = 04/02/16 Pct Recovery = 84% Analysis Date = 03/28/16 Pct Recovery = 84% Analysis Date = 03/28/16 Pct Recovery = 84% Analysis Date = 03/24/16 Pct Recovery = 84% Analysis Date = 03/24/16 Pct Recovery = 84% Analysis Date = 03/19/16 Pct Recovery = 84% Analysis Date = 03/19/16 Pct Recovery = 84% Analysis Date = 03/14/16 Pct Recovery = 84% Analysis Date = 03/14/16 Pct Recovery = 84% Analysis Date = 03/09/16 Pct Recovery = 84% Analysis Date = 03/09/16 Pct Recovery = 84% Analysis Date = 03/04/16 Pct Recovery = 84% Analysis Date = 03/04/16 Pct Recovery = 84% Analysis Date = 02/29/16 Pct Recovery = 84% Analysis Date = 02/29/16 Pct Recovery = 84% Analysis Date = 02/24/16 Pct Recovery = 84% Analysis Date = 02/24/16 Pct Recovery = 84% Analysis Date = 02/19/16 Pct Recovery = 84% Analysis Date = 02/19/16 Pct Recovery = 84% Analysis Date = 02/14/16 Pct Recovery = 84% Analysis Date = 02/14/16 Pct Recovery = 84% Analysis Date = 02/10/16 Pct Recovery = 84% Analysis Date = 02/10/16 Pct Recovery = 84% Analysis Date = 02/05/16 Pct Recovery = 84% Analysis Date = 02/05/16 Pct Recovery = 84% Analysis Date = 01/31/16 Pct Recovery = 85% Analysis Date = 01/31/16 Pct Recovery = 85% Analysis Date = 01/26/16 Pct Recovery = 85% Analysis Date = 01/26/16 Pct Recovery = 85% Analysis Date = 01/21/16 Pct Recovery = 85% Analysis Date = 01/21/16 Pct Recovery = 85% Analysis Date = 01/17/16 Pct Recovery = 85% Analysis Date = 01/17/16 Pct Recovery = 85% Analysis Date = 01/12/16 Pct Recovery = 85% Analysis Date = 01/12/16 Pct Recovery = 85% Analysis Date = 01/07/16 Pct Recovery = 85% Analysis Date = 01/07/16 Pct Recovery = 85% Analysis Date = 01/02/16 Pct Recovery = 85% Analysis Date = 01/02/16 Pct Recovery = 85% Analysis Date = 12/29/15 Pct Recovery = 85% Analysis Date = 12/29/15 Pct Recovery = 85% Analysis Date = 12/24/15 Pct Recovery = 85% Analysis Date = 12/24/15 Pct Recovery = 85% Analysis Date = 12/19/15 Pct Recovery = 85% Analysis Date = 12/19/15 Pct Recovery = 85% Analysis Date = 12/14/15 Pct Recovery = 85% Analysis Date = 12/14/15 Pct Recovery = 85% Analysis Date = 12/09/15 Pct Recovery = 86% Analysis Date = 12/09/15 Pct Recovery = 86% Analysis Date = 12/05/15 Pct Recovery = 86% Analysis Date = 12/05/15 Pct Recovery = 86% Analysis Date = 11/30/15 Pct Recovery = 86% Analysis Date = 11/30/15 Pct Recovery = 86% Analysis Date = 11/25/15 Pct Recovery = 86% Analysis Date = 11/25/15 Pct Recovery = 86% Analysis Date = 11/20/15 Pct Recovery = 86% Analysis Date = 11/20/15 Pct Recovery = 86% Analysis Date = 11/16/15 Pct Recovery = 86% Analysis Date = 11/16/15 Pct Recovery = 86% Analysis Date = 11/11/15 Pct Recovery = 86% Analysis Date = 11/11/15 Pct Recovery = 86% Analysis Date = 11/06/15 Pct Recovery = 86% Analysis Date = 11/06/15 Pct Recovery = 86% Analysis Date = 11/01/15 Pct Recovery = 86% Analysis Date = 11/01/15 Pct Recovery = 86% Analysis Date = 10/27/15 Pct Recovery = 86% Analysis Date = 10/27/15 Pct Recovery = 86% Analysis Date = 10/23/15 Pct Recovery = 86% Analysis Date = 10/23/15 Pct Recovery = 86% Analysis Date = 10/18/15 Pct Recovery = 87% Analysis Date = 10/18/15 Pct Recovery = 87% Analysis Date = 10/13/15 Pct Recovery = 87% Analysis Date = 10/13/15 Pct Recovery = 87% Analysis Date = 10/08/15 Pct Recovery = 87% Analysis Date = 10/08/15 Pct Recovery = 87% Analysis Date = 10/04/15 Pct Recovery = 87% Analysis Date = 10/04/15 Pct Recovery = 87% Analysis Date = 09/29/15 Pct Recovery = 87% Analysis Date = 09/29/15 Pct Recovery = 87% Analysis Date = 09/24/15 Pct Recovery = 87% Analysis Date = 09/24/15 Pct Recovery = 87% Analysis Date = 09/19/15 Pct Recovery = 87% Analysis Date = 09/19/15 Pct Recovery = 87% Analysis Date = 09/14/15 Pct Recovery = 87% Analysis Date = 09/14/15 Pct Recovery = 87% Analysis Date = 09/10/15 Pct Recovery = 87% Analysis Date = 09/10/15 Pct Recovery = 87% Analysis Date = 09/05/15 Pct Recovery = 88% Analysis Date = 09/05/15 Pct Recovery = 88% Analysis Date = 08/31/15 Pct Recovery = 88% Analysis Date = 08/31/15 Pct Recovery = 88% Analysis Date = 08/26/15 Pct Recovery = 88% Analysis Date = 08/26/15 Pct Recovery = 88% Analysis Date = 08/21/15 Pct Recovery = 88% Analysis Date = 08/21/15 Pct Recovery = 88% Analysis Date = 08/17/15 Pct Recovery = 88% Analysis Date = 08/17/15 Pct Recovery = 88% Analysis Date = 08/12/15 Pct Recovery = 88% Analysis Date = 08/12/15 Pct Recovery = 88% Analysis Date = 08/07/15 Pct Recovery = 88% Analysis Date = 08/07/15 Pct Recovery = 88% Analysis Date = 08/02/15 Pct Recovery = 88% Analysis Date = 08/02/15 Pct Recovery = 88% Analysis Date = 07/29/15 Pct Recovery = 88% Analysis Date = 07/29/15 Pct Recovery = 88% Analysis Date = 07/24/15 Pct Recovery = 88% Analysis Date = 07/24/15 Pct Recovery = 88% Analysis Date = 07/19/15 Pct Recovery = 89% Analysis Date = 07/19/15 Pct Recovery = 89% Analysis Date = 07/14/15 Pct Recovery = 89% Analysis Date = 07/14/15 Pct Recovery = 89% Analysis Date = 07/09/15 Pct Recovery = 89% Analysis Date = 07/09/15 Pct Recovery = 89% Analysis Date = 07/05/15 Pct Recovery = 89% Analysis Date = 07/05/15 Pct Recovery = 89% Analysis Date = 06/30/15 Pct Recovery = 89% Analysis Date = 06/30/15 Pct Recovery = 89% Analysis Date = 06/25/15 Pct Recovery = 89% Analysis Date = 06/25/15 Pct Recovery = 89% Analysis Date = 06/20/15 Pct Recovery = 89% Analysis Date = 06/20/15 Pct Recovery = 89% Analysis Date = 06/16/15 Pct Recovery = 89% Analysis Date = 06/16/15 Pct Recovery = 89% Analysis Date = 06/11/15 Pct Recovery = 89% Analysis Date = 06/11/15 Pct Recovery = 89% Analysis Date = 06/06/15 Pct Recovery = 89% Analysis Date = 06/06/15 Pct Recovery = 89% Analysis Date = 06/01/15 Pct Recovery = 90% Analysis Date = 06/01/15 Pct Recovery = 90% Analysis Date = 05/27/15 Pct Recovery = 90% Analysis Date = 05/27/15 Pct Recovery = 90% Analysis Date = 05/23/15 Pct Recovery = 90% Analysis Date = 05/23/15 Pct Recovery = 90% Analysis Date = 05/18/15 Pct Recovery = 90% Analysis Date = 05/18/15 Pct Recovery = 90% Analysis Date = 05/13/15 Pct Recovery = 90% Analysis Date = 05/13/15 Pct Recovery = 90% Analysis Date = 05/08/15 Pct Recovery = 90% Analysis Date = 05/08/15 Pct Recovery = 90% Analysis Date = 05/04/15 Pct Recovery = 90% Analysis Date = 05/04/15 Pct Recovery = 90% Analysis Date = 04/29/15 Pct Recovery = 90% Analysis Date = 04/29/15 Pct Recovery = 90% Analysis Date = 04/24/15 Pct Recovery = 90% Analysis Date = 04/24/15 Pct Recovery = 90% Analysis Date = 04/19/15 Pct Recovery = 90% Analysis Date = 04/19/15 Pct Recovery = 90% Analysis Date = 04/14/15 Pct Recovery = 90% Analysis Date = 04/14/15 Pct Recovery = 90% Analysis Date = 04/10/15 Pct Recovery = 90% Analysis Date = 04/10/15 Pct Recovery = 90% Analysis Date = 04/05/15 Pct Recovery = 90% Analysis Date = 04/05/15 Pct Recovery = 90% Analysis Date = 03/31/15 Pct Recovery = 91% Analysis Date = 03/31/15 Pct Recovery = 91% Analysis Date = 03/26/15 Pct Recovery = 91% Analysis Date = 03/26/15 Pct Recovery = 91% Analysis Date = 03/22/15 Pct Recovery = 91% Analysis Date = 03/22/15 Pct Recovery = 91% Analysis Date = 03/17/15 Pct Recovery = 91% Analysis Date = 03/17/15 Pct Recovery = 91% Analysis Date = 03/12/15 Pct Recovery = 91% Analysis Date = 03/12/15 Pct Recovery = 91% Analysis Date = 03/07/15 Pct Recovery = 91% Analysis Date = 03/07/15 Pct Recovery = 91% Analysis Date = 03/02/15 Pct Recovery = 92% Analysis Date = 03/02/15 Pct Recovery = 92% Analysis Date = 02/26/15 Pct Recovery = 92% Analysis Date = 02/26/15 Pct Recovery = 92% Analysis Date = 02/21/15 Pct Recovery = 92% Analysis Date = 02/21/15 Pct Recovery = 92% Analysis Date = 02/16/15 Pct Recovery = 92% Analysis Date = 02/16/15 Pct Recovery = 92% Analysis Date = 02/11/15 Pct Recovery = 92% Analysis Date = 02/11/15 Pct Recovery = 92% Analysis Date = 02/07/15 Pct Recovery = 92% Analysis Date = 02/07/15 Pct Recovery = 92% Analysis Date = 02/02/15 Pct Recovery = 92% Analysis Date = 02/02/15 Pct Recovery = 92% Analysis Date = 01/28/15 Pct Recovery = 93% Analysis Date = 01/28/15 Pct Recovery = 93% Analysis Date = 01/23/15 Pct Recovery = 93% Analysis Date = 01/23/15 Pct Recovery = 93% Analysis Date = 01/18/15 Pct Recovery = 93% Analysis Date = 01/18/15 Pct Recovery = 93% Analysis Date = 01/14/15 Pct Recovery = 93% Analysis Date = 01/14/15 Pct Recovery = 93% Analysis Date = 01/09/15 Pct Recovery = 93% Analysis Date = 01/09/15 Pct Recovery = 93% Analysis Date = 01/04/15 Pct Recovery = 93% Analysis Date = 01/04/15 Pct Recovery = 93% Analysis Date = 12/30/14 Pct Recovery = 94% Analysis Date = 12/30/14 Pct Recovery = 94% Analysis Date = 12/25/14 Pct Recovery = 94% Analysis Date = 12/25/14 Pct Recovery = 94% Analysis Date = 12/21/14 Pct Recovery = 94% Analysis Date = 12/21/14 Pct Recovery = 94% Analysis Date = 12/16/14 Pct Recovery = 94% Analysis Date = 12/16/14 Pct Recovery = 94% Analysis Date = 12/11/14 Pct Recovery = 94% Analysis Date = 12/11/14 Pct Recovery = 94% Analysis Date = 12/06/14 Pct Recovery = 94% Analysis Date = 12/06/14 Pct Recovery = 94% Analysis Date = 12/02/14 Pct Recovery = 94% Analysis Date = 12/02/14 Pct Recovery = 94% Analysis Date = 11/27/14 Pct Recovery = 94% Analysis Date = 11/27/14 Pct Recovery = 94% Analysis Date = 11/22/14 Pct Recovery = 95% Analysis Date = 11/22/14 Pct Recovery = 95% Analysis Date = 11/17/14 Pct Recovery = 95% Analysis Date = 11/17/14 Pct Recovery = 95% Analysis Date = 11/12/14 Pct Recovery = 95% Analysis Date = 11/12/14 Pct Recovery = 95% Analysis Date = 11/08/14 Pct Recovery = 95% Analysis Date = 11/08/14 Pct Recovery = 95% Analysis Date = 11/03/14 Pct Recovery = 95% Analysis Date = 11/03/14 Pct Recovery = 95% Analysis Date = 10/29/14 Pct Recovery = 95% Analysis Date = 10/29/14 Pct Recovery = 95% Analysis Date = 10/24/14 Pct Recovery = 95% Analysis Date = 10/24/14 Pct Recovery = 95% Analysis Date = 10/20/14 Pct Recovery = 95% Analysis Date = 10/20/14 Pct Recovery = 95% Analysis Date = 10/15/14 Pct Recovery = 95% Analysis Date = 10/15/14 Pct Recovery = 95% Analysis Date = 10/10/14 Pct Recovery = 95% Analysis Date = 10/10/14 Pct Recovery = 95% Analysis Date = 10/05/14 Pct Recovery = 95% Analysis Date = 10/05/14 Pct Recovery = 95% Analysis Date = 09/30/14 Pct Recovery = 95% Analysis Date = 09/30/14 Pct Recovery = 95% Analysis Date = 09/26/14 Pct Recovery = 95% Analysis Date = 09/26/14 Pct Recovery = 95% Analysis Date = 09/21/14 Pct Recovery = 95% Analysis Date = 09/21/14 Pct Recovery = 95% Analysis Date = 09/16/14 Pct Recovery = 95% Analysis Date = 09/16/14 Pct Recovery = 95% Analysis Date = 09/11/14 Pct Recovery = 95% Analysis Date = 09/11/14 Pct Recovery = 95% Analysis Date = 09/07/14 Pct Recovery = 96% Analysis Date = 09/07/14 Pct Recovery = 96% Analysis Date = 09/02/14 Pct Recovery = 96% Analysis Date = 09/02/14 Pct Recovery = 96% Analysis Date = 08/28/14 Pct Recovery = 96% Analysis Date = 08/28/14 Pct Recovery = 96% Analysis Date = 08/23/14 Pct Recovery = 96% Analysis Date = 08/23/14 Pct Recovery = 96% Analysis Date = 08/18/14 Pct Recovery = 96% Analysis Date = 08/18/14 Pct Recovery = 96% Analysis Date = 08/14/14 Pct Recovery = 96% Analysis Date = 08/14/14 Pct Recovery = 96% Analysis Date = 08/09/14 Pct Recovery = 96% Analysis Date = 08/09/14 Pct Recovery = 96% Analysis Date = 08/04/14 Pct Recovery = 96% Analysis Date = 08/04/14 Pct Recovery = 96% Analysis Date = 07/30/14 Pct Recovery = 96% Analysis Date = 07/30/14 Pct Recovery = 96% Analysis Date = 07/26/14 Pct Recovery = 96% Analysis Date = 07/26/14 Pct Recovery = 96% Analysis Date = 07/21/14 Pct Recovery = 96% Analysis Date = 07/21/14 Pct Recovery = 96% Analysis Date = 07/16/14 Pct Recovery = 96% Analysis Date = 07/16/14 Pct Recovery = 96% Analysis Date = 07/11/14 Pct Recovery = 96% Analysis Date = 07/11/14 Pct Recovery = 96% Analysis Date = 07/06/14 Pct Recovery = 96% Analysis Date = 07/06/14 Pct Recovery = 96% Analysis Date = 07/02/14 Pct Recovery = 96% Analysis Date = 07/02/14 Pct Recovery = 96% Analysis Date = 06/27/14 Pct Recovery = 96% Analysis Date = 06/27/14 Pct Recovery = 96% Analysis Date = 06/22/14 Pct Recovery = 96% Analysis Date = 06/22/14 Pct Recovery = 96% Analysis Date = 06/17/14 Pct Recovery = 96% Analysis Date = 06/17/14 Pct Recovery = 96% Analysis Date = 06/13/14 Pct Recovery = 96% Analysis Date = 06/13/14 Pct Recovery = 96% Analysis Date = 06/08/14 Pct Recovery = 96% Analysis Date = 06/08/14 Pct Recovery = 96% Analysis Date = 06/03/14 Pct Recovery = 96% Analysis Date = 06/03/14 Pct Recovery = 96% Analysis Date = 05/29/14 Pct Recovery = 96% Analysis Date = 05/29/14 Pct Recovery = 96% Analysis Date = 05/24/14 Pct Recovery = 96% Analysis Date = 05/24/14 Pct Recovery = 96% Analysis Date = 05/20/14 Pct Recovery = 96% Analysis Date = 05/20/14 Pct Recovery = 96% Analysis Date = 05/15/14 Pct Recovery = 96% Analysis Date = 05/15/14 Pct Recovery = 96% Analysis Date = 05/10/14 Pct Recovery = 96% Analysis Date = 05/10/14 Pct Recovery = 96% Analysis Date = 05/05/14 Pct Recovery = 96% Analysis Date = 05/05/14 Pct Recovery = 96% Analysis Date = 05/01/14 Pct Recovery = 96% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
1,2,3,4-TETRAMETHYLBENZENE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 32 90% 17% 87% 16%
Total 32 90% 17% 87% 16%

Sample Statistics
1,2,3,4-TETRAMETHYLBENZENE

Characteristic N % % Basis
Plotted 32 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 32 .  
False Negatives 0 0% 0 out of 32
Not Spiked 41 .  
False Positives 0 0% 0 out of 41

BQS OBSP Determination:
1,2,3,5-TETRAMETHYLBENZENE
METHOD: 4440 , TESTIDCODE: 50000GCM66
Open Data Set

Analysis Date = 12/16/16 SpikeMix = NSI 041816AVOC: 40 µl & ChemService 5082900: 40 µl Pct Recovery = 84% Analysis Date = 12/12/16 SpikeMix = Accu 216041125: 40 µl & Crescent 03FF058: 40 µl Pct Recovery = 105% Analysis Date = 08/04/16 SpikeMix = Crescent 03FF058: 40 µl & Supelco LC20141V: 40 µl Pct Recovery = 85% Analysis Date = 07/14/16 SpikeMix = Accu 216041125: 40 µl & NSI 041816AVOC: 40 µl Pct Recovery = 85% Analysis Date = 11/21/16 SpikeMix = Crescent 03FF058: 25 µl & Supelco LC20141V: 25 µl Pct Recovery = 94% Analysis Date = 08/26/16 SpikeMix = NSI 041816AVOC: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 78% Analysis Date = 06/30/16 SpikeMix = Crescent 03FF058: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 81% Analysis Date = 06/21/16 SpikeMix = Phenova B20160319: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 90% Analysis Date = 05/24/16 SpikeMix = Accu 216041125: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 90% Analysis Date = 04/09/15 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 81% Analysis Date = 03/06/15 SpikeMix = ERA 0227-14-06.1A: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 74% Analysis Date = 11/14/14 SpikeMix = Crescent 03DD004: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 83% Analysis Date = 08/16/14 SpikeMix = ERA 0227-14-06.1A: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 102% Analysis Date = 07/01/14 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 82% Analysis Date = 11/22/14 SpikeMix = NSI 032614: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 84% Analysis Date = 06/10/14 SpikeMix = Crescent 03DD004: 20 µl & NSI 032614: 20 µl Pct Recovery = 72% Analysis Date = 06/10/14 SpikeMix = NSI 032614: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 74% Analysis Date = 05/01/14 SpikeMix = Accu 214031115: 20 µl & NSI 032614: 20 µl Pct Recovery = 83% Analysis Date = 08/15/15 SpikeMix = Supelco LC13545: 25 µl & Crescent 04EE008: 25 µl Pct Recovery = 87% Analysis Date = 06/16/15 SpikeMix = ERA 0406-15-03: 25 µl & Supelco LC13545: 25 µl Pct Recovery = 86% Analysis Date = 10/13/16 SpikeMix = Accu 216041125: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 93% Analysis Date = 10/13/16 SpikeMix = NSI 041816AVOC: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 88% Analysis Date = 09/28/16 SpikeMix = Crescent 03FF058: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 88% Analysis Date = 09/08/16 SpikeMix = Phenova B20160319: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 81% Analysis Date = 08/20/16 SpikeMix = Accu 216041125: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 100% Analysis Date = 07/29/16 SpikeMix = Phenova B20160319: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 86% Analysis Date = 06/10/16 SpikeMix = NSI 041816AVOC: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 79% Analysis Date = 04/26/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 95% Analysis Date = 02/05/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 87% Analysis Date = 11/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 99% Analysis Date = 10/16/15 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 95% Analysis Date = 05/09/15 SpikeMix = Spex Organics EN150428007: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 88% Analysis Date = 04/02/16 SpikeMix = Supelco LC13545: 15 µl & Accu 215041380: 15 µl Pct Recovery = 78% Analysis Date = 12/18/15 SpikeMix = Supelco LC13545: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 93% Analysis Date = 01/13/15 SpikeMix = Accu 214031115: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 104% Analysis Date = 10/21/14 SpikeMix = ERA 0227-14-06.1A: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 85% Analysis Date = 10/04/14 SpikeMix = Crescent 03DD004: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 87% Analysis Date = 07/11/14 SpikeMix = Spex Organics C1140417015: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 87% Analysis Date = 09/09/14 SpikeMix = Accu 214031115: 10 µl & NSI 032614: 10 µl Pct Recovery = 147% Analysis Date = 09/09/14 SpikeMix = NSI 032614: 10 µl & Spex Organics C1140417015: 10 µl Pct Recovery = 146% Analysis Date = 07/29/14 SpikeMix = Crescent 03DD004: 10 µl & NSI 032614: 10 µl Pct Recovery = 122% Analysis Date = 02/18/16 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 82% Analysis Date = 11/12/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 94% Analysis Date = 09/03/15 SpikeMix = NSI 050515AVOC: 10 µl & Spex Organics EN150428007: 10 µl Pct Recovery = 104% Analysis Date = 05/21/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 107% Analysis Date = 05/13/16 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 87% Analysis Date = 03/17/16 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 67% Analysis Date = 12/10/15 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 90% Analysis Date = 06/27/15 SpikeMix = ERA 0406-15-03: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 116% Analysis Date = 05/09/15 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 91% Analysis Date = 12/15/16 Pct Recovery = 90% Analysis Date = 12/11/16 Pct Recovery = 90% Analysis Date = 12/11/16 Pct Recovery = 90% Analysis Date = 12/06/16 Pct Recovery = 90% Analysis Date = 12/06/16 Pct Recovery = 90% Analysis Date = 12/01/16 Pct Recovery = 90% Analysis Date = 12/01/16 Pct Recovery = 90% Analysis Date = 11/26/16 Pct Recovery = 90% Analysis Date = 11/26/16 Pct Recovery = 90% Analysis Date = 11/21/16 Pct Recovery = 90% Analysis Date = 11/21/16 Pct Recovery = 90% Analysis Date = 11/17/16 Pct Recovery = 89% Analysis Date = 11/17/16 Pct Recovery = 89% Analysis Date = 11/12/16 Pct Recovery = 89% Analysis Date = 11/12/16 Pct Recovery = 89% Analysis Date = 11/07/16 Pct Recovery = 89% Analysis Date = 11/07/16 Pct Recovery = 89% Analysis Date = 11/02/16 Pct Recovery = 89% Analysis Date = 11/02/16 Pct Recovery = 89% Analysis Date = 10/28/16 Pct Recovery = 89% Analysis Date = 10/28/16 Pct Recovery = 89% Analysis Date = 10/24/16 Pct Recovery = 89% Analysis Date = 10/24/16 Pct Recovery = 89% Analysis Date = 10/19/16 Pct Recovery = 89% Analysis Date = 10/19/16 Pct Recovery = 89% Analysis Date = 10/14/16 Pct Recovery = 89% Analysis Date = 10/14/16 Pct Recovery = 89% Analysis Date = 10/09/16 Pct Recovery = 89% Analysis Date = 10/09/16 Pct Recovery = 89% Analysis Date = 10/04/16 Pct Recovery = 89% Analysis Date = 10/04/16 Pct Recovery = 89% Analysis Date = 09/30/16 Pct Recovery = 88% Analysis Date = 09/30/16 Pct Recovery = 88% Analysis Date = 09/25/16 Pct Recovery = 88% Analysis Date = 09/25/16 Pct Recovery = 88% Analysis Date = 09/20/16 Pct Recovery = 88% Analysis Date = 09/20/16 Pct Recovery = 88% Analysis Date = 09/15/16 Pct Recovery = 88% Analysis Date = 09/15/16 Pct Recovery = 88% Analysis Date = 09/10/16 Pct Recovery = 88% Analysis Date = 09/10/16 Pct Recovery = 88% Analysis Date = 09/06/16 Pct Recovery = 88% Analysis Date = 09/06/16 Pct Recovery = 88% Analysis Date = 09/01/16 Pct Recovery = 88% Analysis Date = 09/01/16 Pct Recovery = 88% Analysis Date = 08/27/16 Pct Recovery = 88% Analysis Date = 08/27/16 Pct Recovery = 88% Analysis Date = 08/22/16 Pct Recovery = 88% Analysis Date = 08/22/16 Pct Recovery = 88% Analysis Date = 08/17/16 Pct Recovery = 88% Analysis Date = 08/17/16 Pct Recovery = 88% Analysis Date = 08/13/16 Pct Recovery = 88% Analysis Date = 08/13/16 Pct Recovery = 88% Analysis Date = 08/08/16 Pct Recovery = 88% Analysis Date = 08/08/16 Pct Recovery = 88% Analysis Date = 08/03/16 Pct Recovery = 88% Analysis Date = 08/03/16 Pct Recovery = 88% Analysis Date = 07/29/16 Pct Recovery = 87% Analysis Date = 07/29/16 Pct Recovery = 87% Analysis Date = 07/24/16 Pct Recovery = 87% Analysis Date = 07/24/16 Pct Recovery = 87% Analysis Date = 07/20/16 Pct Recovery = 87% Analysis Date = 07/20/16 Pct Recovery = 87% Analysis Date = 07/15/16 Pct Recovery = 87% Analysis Date = 07/15/16 Pct Recovery = 87% Analysis Date = 07/10/16 Pct Recovery = 87% Analysis Date = 07/10/16 Pct Recovery = 87% Analysis Date = 07/05/16 Pct Recovery = 87% Analysis Date = 07/05/16 Pct Recovery = 87% Analysis Date = 06/30/16 Pct Recovery = 87% Analysis Date = 06/30/16 Pct Recovery = 87% Analysis Date = 06/26/16 Pct Recovery = 87% Analysis Date = 06/26/16 Pct Recovery = 87% Analysis Date = 06/21/16 Pct Recovery = 87% Analysis Date = 06/21/16 Pct Recovery = 87% Analysis Date = 06/16/16 Pct Recovery = 87% Analysis Date = 06/16/16 Pct Recovery = 87% Analysis Date = 06/11/16 Pct Recovery = 87% Analysis Date = 06/11/16 Pct Recovery = 87% Analysis Date = 06/06/16 Pct Recovery = 87% Analysis Date = 06/06/16 Pct Recovery = 87% Analysis Date = 06/02/16 Pct Recovery = 87% Analysis Date = 06/02/16 Pct Recovery = 87% Analysis Date = 05/28/16 Pct Recovery = 87% Analysis Date = 05/28/16 Pct Recovery = 87% Analysis Date = 05/23/16 Pct Recovery = 87% Analysis Date = 05/23/16 Pct Recovery = 87% Analysis Date = 05/18/16 Pct Recovery = 87% Analysis Date = 05/18/16 Pct Recovery = 87% Analysis Date = 05/13/16 Pct Recovery = 87% Analysis Date = 05/13/16 Pct Recovery = 87% Analysis Date = 05/09/16 Pct Recovery = 87% Analysis Date = 05/09/16 Pct Recovery = 87% Analysis Date = 05/04/16 Pct Recovery = 87% Analysis Date = 05/04/16 Pct Recovery = 87% Analysis Date = 04/29/16 Pct Recovery = 87% Analysis Date = 04/29/16 Pct Recovery = 87% Analysis Date = 04/24/16 Pct Recovery = 87% Analysis Date = 04/24/16 Pct Recovery = 87% Analysis Date = 04/19/16 Pct Recovery = 87% Analysis Date = 04/19/16 Pct Recovery = 87% Analysis Date = 04/15/16 Pct Recovery = 87% Analysis Date = 04/15/16 Pct Recovery = 87% Analysis Date = 04/10/16 Pct Recovery = 87% Analysis Date = 04/10/16 Pct Recovery = 87% Analysis Date = 04/05/16 Pct Recovery = 87% Analysis Date = 04/05/16 Pct Recovery = 87% Analysis Date = 03/31/16 Pct Recovery = 87% Analysis Date = 03/31/16 Pct Recovery = 87% Analysis Date = 03/26/16 Pct Recovery = 87% Analysis Date = 03/26/16 Pct Recovery = 87% Analysis Date = 03/22/16 Pct Recovery = 87% Analysis Date = 03/22/16 Pct Recovery = 87% Analysis Date = 03/17/16 Pct Recovery = 87% Analysis Date = 03/17/16 Pct Recovery = 87% Analysis Date = 03/12/16 Pct Recovery = 87% Analysis Date = 03/12/16 Pct Recovery = 87% Analysis Date = 03/07/16 Pct Recovery = 88% Analysis Date = 03/07/16 Pct Recovery = 88% Analysis Date = 03/02/16 Pct Recovery = 88% Analysis Date = 03/02/16 Pct Recovery = 88% Analysis Date = 02/27/16 Pct Recovery = 88% Analysis Date = 02/27/16 Pct Recovery = 88% Analysis Date = 02/22/16 Pct Recovery = 88% Analysis Date = 02/22/16 Pct Recovery = 88% Analysis Date = 02/17/16 Pct Recovery = 88% Analysis Date = 02/17/16 Pct Recovery = 88% Analysis Date = 02/12/16 Pct Recovery = 88% Analysis Date = 02/12/16 Pct Recovery = 88% Analysis Date = 02/07/16 Pct Recovery = 89% Analysis Date = 02/07/16 Pct Recovery = 89% Analysis Date = 02/03/16 Pct Recovery = 89% Analysis Date = 02/03/16 Pct Recovery = 89% Analysis Date = 01/29/16 Pct Recovery = 89% Analysis Date = 01/29/16 Pct Recovery = 89% Analysis Date = 01/24/16 Pct Recovery = 89% Analysis Date = 01/24/16 Pct Recovery = 89% Analysis Date = 01/19/16 Pct Recovery = 89% Analysis Date = 01/19/16 Pct Recovery = 89% Analysis Date = 01/14/16 Pct Recovery = 89% Analysis Date = 01/14/16 Pct Recovery = 89% Analysis Date = 01/10/16 Pct Recovery = 89% Analysis Date = 01/10/16 Pct Recovery = 89% Analysis Date = 01/05/16 Pct Recovery = 90% Analysis Date = 01/05/16 Pct Recovery = 90% Analysis Date = 12/31/15 Pct Recovery = 90% Analysis Date = 12/31/15 Pct Recovery = 90% Analysis Date = 12/26/15 Pct Recovery = 90% Analysis Date = 12/26/15 Pct Recovery = 90% Analysis Date = 12/21/15 Pct Recovery = 90% Analysis Date = 12/21/15 Pct Recovery = 90% Analysis Date = 12/17/15 Pct Recovery = 90% Analysis Date = 12/17/15 Pct Recovery = 90% Analysis Date = 12/12/15 Pct Recovery = 90% Analysis Date = 12/12/15 Pct Recovery = 90% Analysis Date = 12/07/15 Pct Recovery = 90% Analysis Date = 12/07/15 Pct Recovery = 90% Analysis Date = 12/02/15 Pct Recovery = 90% Analysis Date = 12/02/15 Pct Recovery = 90% Analysis Date = 11/27/15 Pct Recovery = 91% Analysis Date = 11/27/15 Pct Recovery = 91% Analysis Date = 11/23/15 Pct Recovery = 91% Analysis Date = 11/23/15 Pct Recovery = 91% Analysis Date = 11/18/15 Pct Recovery = 91% Analysis Date = 11/18/15 Pct Recovery = 91% Analysis Date = 11/13/15 Pct Recovery = 91% Analysis Date = 11/13/15 Pct Recovery = 91% Analysis Date = 11/08/15 Pct Recovery = 91% Analysis Date = 11/08/15 Pct Recovery = 91% Analysis Date = 11/03/15 Pct Recovery = 91% Analysis Date = 11/03/15 Pct Recovery = 91% Analysis Date = 10/30/15 Pct Recovery = 91% Analysis Date = 10/30/15 Pct Recovery = 91% Analysis Date = 10/25/15 Pct Recovery = 91% Analysis Date = 10/25/15 Pct Recovery = 91% Analysis Date = 10/20/15 Pct Recovery = 92% Analysis Date = 10/20/15 Pct Recovery = 92% Analysis Date = 10/15/15 Pct Recovery = 92% Analysis Date = 10/15/15 Pct Recovery = 92% Analysis Date = 10/10/15 Pct Recovery = 92% Analysis Date = 10/10/15 Pct Recovery = 92% Analysis Date = 10/06/15 Pct Recovery = 92% Analysis Date = 10/06/15 Pct Recovery = 92% Analysis Date = 10/01/15 Pct Recovery = 92% Analysis Date = 10/01/15 Pct Recovery = 92% Analysis Date = 09/26/15 Pct Recovery = 92% Analysis Date = 09/26/15 Pct Recovery = 92% Analysis Date = 09/21/15 Pct Recovery = 92% Analysis Date = 09/21/15 Pct Recovery = 92% Analysis Date = 09/16/15 Pct Recovery = 92% Analysis Date = 09/16/15 Pct Recovery = 92% Analysis Date = 09/12/15 Pct Recovery = 92% Analysis Date = 09/12/15 Pct Recovery = 92% Analysis Date = 09/07/15 Pct Recovery = 92% Analysis Date = 09/07/15 Pct Recovery = 92% Analysis Date = 09/02/15 Pct Recovery = 92% Analysis Date = 09/02/15 Pct Recovery = 92% Analysis Date = 08/28/15 Pct Recovery = 92% Analysis Date = 08/28/15 Pct Recovery = 92% Analysis Date = 08/23/15 Pct Recovery = 92% Analysis Date = 08/23/15 Pct Recovery = 92% Analysis Date = 08/19/15 Pct Recovery = 93% Analysis Date = 08/19/15 Pct Recovery = 93% Analysis Date = 08/14/15 Pct Recovery = 93% Analysis Date = 08/14/15 Pct Recovery = 93% Analysis Date = 08/09/15 Pct Recovery = 93% Analysis Date = 08/09/15 Pct Recovery = 93% Analysis Date = 08/04/15 Pct Recovery = 93% Analysis Date = 08/04/15 Pct Recovery = 93% Analysis Date = 07/30/15 Pct Recovery = 93% Analysis Date = 07/30/15 Pct Recovery = 93% Analysis Date = 07/26/15 Pct Recovery = 93% Analysis Date = 07/26/15 Pct Recovery = 93% Analysis Date = 07/21/15 Pct Recovery = 93% Analysis Date = 07/21/15 Pct Recovery = 93% Analysis Date = 07/16/15 Pct Recovery = 93% Analysis Date = 07/16/15 Pct Recovery = 93% Analysis Date = 07/11/15 Pct Recovery = 93% Analysis Date = 07/11/15 Pct Recovery = 93% Analysis Date = 07/06/15 Pct Recovery = 93% Analysis Date = 07/06/15 Pct Recovery = 93% Analysis Date = 07/02/15 Pct Recovery = 93% Analysis Date = 07/02/15 Pct Recovery = 93% Analysis Date = 06/27/15 Pct Recovery = 93% Analysis Date = 06/27/15 Pct Recovery = 93% Analysis Date = 06/22/15 Pct Recovery = 93% Analysis Date = 06/22/15 Pct Recovery = 93% Analysis Date = 06/17/15 Pct Recovery = 93% Analysis Date = 06/17/15 Pct Recovery = 93% Analysis Date = 06/12/15 Pct Recovery = 94% Analysis Date = 06/12/15 Pct Recovery = 94% Analysis Date = 06/08/15 Pct Recovery = 94% Analysis Date = 06/08/15 Pct Recovery = 94% Analysis Date = 06/03/15 Pct Recovery = 94% Analysis Date = 06/03/15 Pct Recovery = 94% Analysis Date = 05/29/15 Pct Recovery = 94% Analysis Date = 05/29/15 Pct Recovery = 94% Analysis Date = 05/24/15 Pct Recovery = 94% Analysis Date = 05/24/15 Pct Recovery = 94% Analysis Date = 05/19/15 Pct Recovery = 94% Analysis Date = 05/19/15 Pct Recovery = 94% Analysis Date = 05/15/15 Pct Recovery = 94% Analysis Date = 05/15/15 Pct Recovery = 94% Analysis Date = 05/10/15 Pct Recovery = 94% Analysis Date = 05/10/15 Pct Recovery = 94% Analysis Date = 05/05/15 Pct Recovery = 94% Analysis Date = 05/05/15 Pct Recovery = 94% Analysis Date = 04/30/15 Pct Recovery = 94% Analysis Date = 04/30/15 Pct Recovery = 94% Analysis Date = 04/25/15 Pct Recovery = 94% Analysis Date = 04/25/15 Pct Recovery = 94% Analysis Date = 04/21/15 Pct Recovery = 94% Analysis Date = 04/21/15 Pct Recovery = 94% Analysis Date = 04/16/15 Pct Recovery = 94% Analysis Date = 04/16/15 Pct Recovery = 94% Analysis Date = 04/11/15 Pct Recovery = 94% Analysis Date = 04/11/15 Pct Recovery = 94% Analysis Date = 04/06/15 Pct Recovery = 94% Analysis Date = 04/06/15 Pct Recovery = 94% Analysis Date = 04/01/15 Pct Recovery = 94% Analysis Date = 04/01/15 Pct Recovery = 94% Analysis Date = 03/28/15 Pct Recovery = 94% Analysis Date = 03/28/15 Pct Recovery = 94% Analysis Date = 03/23/15 Pct Recovery = 94% Analysis Date = 03/23/15 Pct Recovery = 94% Analysis Date = 03/18/15 Pct Recovery = 94% Analysis Date = 03/18/15 Pct Recovery = 94% Analysis Date = 03/13/15 Pct Recovery = 95% Analysis Date = 03/13/15 Pct Recovery = 95% Analysis Date = 03/08/15 Pct Recovery = 95% Analysis Date = 03/08/15 Pct Recovery = 95% Analysis Date = 03/04/15 Pct Recovery = 95% Analysis Date = 03/04/15 Pct Recovery = 95% Analysis Date = 02/27/15 Pct Recovery = 95% Analysis Date = 02/27/15 Pct Recovery = 95% Analysis Date = 02/22/15 Pct Recovery = 95% Analysis Date = 02/22/15 Pct Recovery = 95% Analysis Date = 02/17/15 Pct Recovery = 95% Analysis Date = 02/17/15 Pct Recovery = 95% Analysis Date = 02/12/15 Pct Recovery = 95% Analysis Date = 02/12/15 Pct Recovery = 95% Analysis Date = 02/08/15 Pct Recovery = 95% Analysis Date = 02/08/15 Pct Recovery = 95% Analysis Date = 02/03/15 Pct Recovery = 95% Analysis Date = 02/03/15 Pct Recovery = 95% Analysis Date = 01/29/15 Pct Recovery = 95% Analysis Date = 01/29/15 Pct Recovery = 95% Analysis Date = 01/24/15 Pct Recovery = 95% Analysis Date = 01/24/15 Pct Recovery = 95% Analysis Date = 01/19/15 Pct Recovery = 95% Analysis Date = 01/19/15 Pct Recovery = 95% Analysis Date = 01/15/15 Pct Recovery = 95% Analysis Date = 01/15/15 Pct Recovery = 95% Analysis Date = 01/10/15 Pct Recovery = 95% Analysis Date = 01/10/15 Pct Recovery = 95% Analysis Date = 01/05/15 Pct Recovery = 95% Analysis Date = 01/05/15 Pct Recovery = 95% Analysis Date = 12/31/14 Pct Recovery = 95% Analysis Date = 12/31/14 Pct Recovery = 95% Analysis Date = 12/26/14 Pct Recovery = 95% Analysis Date = 12/26/14 Pct Recovery = 95% Analysis Date = 12/22/14 Pct Recovery = 95% Analysis Date = 12/22/14 Pct Recovery = 95% Analysis Date = 12/17/14 Pct Recovery = 95% Analysis Date = 12/17/14 Pct Recovery = 95% Analysis Date = 12/12/14 Pct Recovery = 95% Analysis Date = 12/12/14 Pct Recovery = 95% Analysis Date = 12/07/14 Pct Recovery = 95% Analysis Date = 12/07/14 Pct Recovery = 95% Analysis Date = 12/02/14 Pct Recovery = 95% Analysis Date = 12/02/14 Pct Recovery = 95% Analysis Date = 11/28/14 Pct Recovery = 95% Analysis Date = 11/28/14 Pct Recovery = 95% Analysis Date = 11/23/14 Pct Recovery = 96% Analysis Date = 11/23/14 Pct Recovery = 96% Analysis Date = 11/18/14 Pct Recovery = 96% Analysis Date = 11/18/14 Pct Recovery = 96% Analysis Date = 11/13/14 Pct Recovery = 96% Analysis Date = 11/13/14 Pct Recovery = 96% Analysis Date = 11/08/14 Pct Recovery = 95% Analysis Date = 11/08/14 Pct Recovery = 95% Analysis Date = 11/04/14 Pct Recovery = 95% Analysis Date = 11/04/14 Pct Recovery = 95% Analysis Date = 10/30/14 Pct Recovery = 95% Analysis Date = 10/30/14 Pct Recovery = 95% Analysis Date = 10/25/14 Pct Recovery = 95% Analysis Date = 10/25/14 Pct Recovery = 95% Analysis Date = 10/20/14 Pct Recovery = 95% Analysis Date = 10/20/14 Pct Recovery = 95% Analysis Date = 10/15/14 Pct Recovery = 95% Analysis Date = 10/15/14 Pct Recovery = 95% Analysis Date = 10/11/14 Pct Recovery = 95% Analysis Date = 10/11/14 Pct Recovery = 95% Analysis Date = 10/06/14 Pct Recovery = 95% Analysis Date = 10/06/14 Pct Recovery = 95% Analysis Date = 10/01/14 Pct Recovery = 95% Analysis Date = 10/01/14 Pct Recovery = 95% Analysis Date = 09/26/14 Pct Recovery = 95% Analysis Date = 09/26/14 Pct Recovery = 95% Analysis Date = 09/21/14 Pct Recovery = 95% Analysis Date = 09/21/14 Pct Recovery = 95% Analysis Date = 09/17/14 Pct Recovery = 95% Analysis Date = 09/17/14 Pct Recovery = 95% Analysis Date = 09/12/14 Pct Recovery = 95% Analysis Date = 09/12/14 Pct Recovery = 95% Analysis Date = 09/07/14 Pct Recovery = 95% Analysis Date = 09/07/14 Pct Recovery = 95% Analysis Date = 09/02/14 Pct Recovery = 95% Analysis Date = 09/02/14 Pct Recovery = 95% Analysis Date = 08/28/14 Pct Recovery = 95% Analysis Date = 08/28/14 Pct Recovery = 95% Analysis Date = 08/24/14 Pct Recovery = 95% Analysis Date = 08/24/14 Pct Recovery = 95% Analysis Date = 08/19/14 Pct Recovery = 95% Analysis Date = 08/19/14 Pct Recovery = 95% Analysis Date = 08/14/14 Pct Recovery = 95% Analysis Date = 08/14/14 Pct Recovery = 95% Analysis Date = 08/09/14 Pct Recovery = 95% Analysis Date = 08/09/14 Pct Recovery = 95% Analysis Date = 08/04/14 Pct Recovery = 95% Analysis Date = 08/04/14 Pct Recovery = 95% Analysis Date = 07/31/14 Pct Recovery = 95% Analysis Date = 07/31/14 Pct Recovery = 95% Analysis Date = 07/26/14 Pct Recovery = 95% Analysis Date = 07/26/14 Pct Recovery = 95% Analysis Date = 07/21/14 Pct Recovery = 95% Analysis Date = 07/21/14 Pct Recovery = 95% Analysis Date = 07/16/14 Pct Recovery = 95% Analysis Date = 07/16/14 Pct Recovery = 95% Analysis Date = 07/11/14 Pct Recovery = 95% Analysis Date = 07/11/14 Pct Recovery = 95% Analysis Date = 07/07/14 Pct Recovery = 95% Analysis Date = 07/07/14 Pct Recovery = 95% Analysis Date = 07/02/14 Pct Recovery = 95% Analysis Date = 07/02/14 Pct Recovery = 95% Analysis Date = 06/27/14 Pct Recovery = 95% Analysis Date = 06/27/14 Pct Recovery = 95% Analysis Date = 06/22/14 Pct Recovery = 95% Analysis Date = 06/22/14 Pct Recovery = 95% Analysis Date = 06/17/14 Pct Recovery = 95% Analysis Date = 06/17/14 Pct Recovery = 95% Analysis Date = 06/13/14 Pct Recovery = 95% Analysis Date = 06/13/14 Pct Recovery = 95% Analysis Date = 06/08/14 Pct Recovery = 95% Analysis Date = 06/08/14 Pct Recovery = 95% Analysis Date = 06/03/14 Pct Recovery = 95% Analysis Date = 06/03/14 Pct Recovery = 95% Analysis Date = 05/29/14 Pct Recovery = 95% Analysis Date = 05/29/14 Pct Recovery = 95% Analysis Date = 05/24/14 Pct Recovery = 95% Analysis Date = 05/24/14 Pct Recovery = 95% Analysis Date = 05/20/14 Pct Recovery = 95% Analysis Date = 05/20/14 Pct Recovery = 95% Analysis Date = 05/15/14 Pct Recovery = 95% Analysis Date = 05/15/14 Pct Recovery = 95% Analysis Date = 05/10/14 Pct Recovery = 95% Analysis Date = 05/10/14 Pct Recovery = 95% Analysis Date = 05/05/14 Pct Recovery = 95% Analysis Date = 05/05/14 Pct Recovery = 95% Analysis Date = 05/01/14 Pct Recovery = 95% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
1,2,3,5-TETRAMETHYLBENZENE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 50 91% 16% 87% 9%
Total 50 91% 16% 87% 9%

Sample Statistics
1,2,3,5-TETRAMETHYLBENZENE

Characteristic N % % Basis
Plotted 50 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 50 .  
False Negatives 0 0% 0 out of 50
Not Spiked 22 .  
False Positives 0 0% 0 out of 22

BQS OBSP Determination:
1,2,3-TRICHLOROBENZENE
METHOD: 4440 , TESTIDCODE: 77613GCM66
Open Data Set

Analysis Date = 12/12/16 SpikeMix = Accu 216041125: 40 µl & Crescent 03FF058: 40 µl Pct Recovery = 91% Analysis Date = 08/04/16 SpikeMix = Crescent 03FF058: 40 µl & Supelco LC20141V: 40 µl Pct Recovery = 86% Analysis Date = 11/21/16 SpikeMix = Crescent 03FF058: 25 µl & Supelco LC20141V: 25 µl Pct Recovery = 88% Analysis Date = 06/30/16 SpikeMix = Crescent 03FF058: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 84% Analysis Date = 06/21/16 SpikeMix = Phenova B20160319: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 92% Analysis Date = 05/24/16 SpikeMix = Accu 216041125: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 84% Analysis Date = 03/06/15 SpikeMix = ERA 0227-14-06.1A: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 88% Analysis Date = 12/17/14 SpikeMix = Supelco LC06438: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 89% Analysis Date = 09/21/14 SpikeMix = Supelco LC06438: 20 µl Pct Recovery = 78% Analysis Date = 06/10/14 SpikeMix = NSI 032614: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 96% Analysis Date = 03/19/15 SpikeMix = Spex Organics C1140417015: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 103% Analysis Date = 11/22/14 SpikeMix = NSI 032614: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 102% Analysis Date = 08/19/14 SpikeMix = Spex Organics C1140417015: 20 µl & Accu 214031115: 20 µl Pct Recovery = 95% Analysis Date = 08/16/14 SpikeMix = ERA 0227-14-06.1A: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 86% Analysis Date = 09/29/15 SpikeMix = Accu 215041380: 25 µl & ERA 0406-15-03: 25 µl Pct Recovery = 105% Analysis Date = 06/16/15 SpikeMix = ERA 0406-15-03: 25 µl & Supelco LC13545: 25 µl Pct Recovery = 93% Analysis Date = 07/13/15 SpikeMix = Crescent 04EE008: 25 µl & NSI 050515AVOC: 25 µl Pct Recovery = 84% Analysis Date = 09/28/16 SpikeMix = Crescent 03FF058: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 81% Analysis Date = 09/08/16 SpikeMix = Phenova B20160319: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 83% Analysis Date = 08/20/16 SpikeMix = Accu 216041125: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 93% Analysis Date = 04/26/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 108% Analysis Date = 03/04/16 SpikeMix = Accu 215041380: 15 µl & ERA 0406-15-03: 15 µl Pct Recovery = 86% Analysis Date = 02/05/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 86% Analysis Date = 10/16/15 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 107% Analysis Date = 11/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 101% Analysis Date = 10/17/15 SpikeMix = Crescent 04EE008: 15 µl & NSI 050515AVOC: 15 µl Pct Recovery = 98% Analysis Date = 06/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Accu 215041380: 15 µl Pct Recovery = 85% Analysis Date = 10/21/14 SpikeMix = ERA 0227-14-06.1A: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 95% Analysis Date = 06/18/14 SpikeMix = Supelco LC06438: 10 µl & Accu 214031115: 10 µl Pct Recovery = 90% Analysis Date = 05/30/14 SpikeMix = NSI 032614: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 71% Analysis Date = 05/03/14 SpikeMix = Crescent 03DD004: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 91% Analysis Date = 11/06/14 SpikeMix = Spex Organics C1140417015: 10 µl & Crescent 03DD004: 10 µl Pct Recovery = 103% Analysis Date = 09/09/14 SpikeMix = NSI 032614: 10 µl & Spex Organics C1140417015: 10 µl Pct Recovery = 103% Analysis Date = 07/23/14 SpikeMix = Spex Organics C1140417015: 10 µl & Accu 214031115: 10 µl Pct Recovery = 98% Analysis Date = 07/11/14 SpikeMix = Spex Organics C1140417015: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 96% Analysis Date = 11/20/15 SpikeMix = Accu 215041380: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 90% Analysis Date = 07/31/15 SpikeMix = Crescent 04EE008: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 93% Analysis Date = 06/27/15 SpikeMix = ERA 0406-15-03: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 96% Analysis Date = 03/17/16 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 79% Analysis Date = 01/27/16 SpikeMix = Crescent 04EE008: 10 µl & NSI 050515AVOC: 10 µl Pct Recovery = 87% Analysis Date = 12/10/15 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 88% Analysis Date = 09/03/15 SpikeMix = NSI 050515AVOC: 10 µl & Spex Organics EN150428007: 10 µl Pct Recovery = 87% Analysis Date = 12/12/16 Pct Recovery = 86% Analysis Date = 12/07/16 Pct Recovery = 86% Analysis Date = 12/07/16 Pct Recovery = 86% Analysis Date = 12/02/16 Pct Recovery = 86% Analysis Date = 12/02/16 Pct Recovery = 86% Analysis Date = 11/27/16 Pct Recovery = 86% Analysis Date = 11/27/16 Pct Recovery = 86% Analysis Date = 11/22/16 Pct Recovery = 86% Analysis Date = 11/22/16 Pct Recovery = 86% Analysis Date = 11/18/16 Pct Recovery = 86% Analysis Date = 11/18/16 Pct Recovery = 86% Analysis Date = 11/13/16 Pct Recovery = 86% Analysis Date = 11/13/16 Pct Recovery = 86% Analysis Date = 11/08/16 Pct Recovery = 86% Analysis Date = 11/08/16 Pct Recovery = 86% Analysis Date = 11/03/16 Pct Recovery = 86% Analysis Date = 11/03/16 Pct Recovery = 86% Analysis Date = 10/30/16 Pct Recovery = 87% Analysis Date = 10/30/16 Pct Recovery = 87% Analysis Date = 10/25/16 Pct Recovery = 87% Analysis Date = 10/25/16 Pct Recovery = 87% Analysis Date = 10/20/16 Pct Recovery = 87% Analysis Date = 10/20/16 Pct Recovery = 87% Analysis Date = 10/15/16 Pct Recovery = 87% Analysis Date = 10/15/16 Pct Recovery = 87% Analysis Date = 10/10/16 Pct Recovery = 87% Analysis Date = 10/10/16 Pct Recovery = 87% Analysis Date = 10/06/16 Pct Recovery = 87% Analysis Date = 10/06/16 Pct Recovery = 87% Analysis Date = 10/01/16 Pct Recovery = 87% Analysis Date = 10/01/16 Pct Recovery = 87% Analysis Date = 09/26/16 Pct Recovery = 87% Analysis Date = 09/26/16 Pct Recovery = 87% Analysis Date = 09/21/16 Pct Recovery = 87% Analysis Date = 09/21/16 Pct Recovery = 87% Analysis Date = 09/17/16 Pct Recovery = 87% Analysis Date = 09/17/16 Pct Recovery = 87% Analysis Date = 09/12/16 Pct Recovery = 87% Analysis Date = 09/12/16 Pct Recovery = 87% Analysis Date = 09/07/16 Pct Recovery = 87% Analysis Date = 09/07/16 Pct Recovery = 87% Analysis Date = 09/02/16 Pct Recovery = 87% Analysis Date = 09/02/16 Pct Recovery = 87% Analysis Date = 08/29/16 Pct Recovery = 87% Analysis Date = 08/29/16 Pct Recovery = 87% Analysis Date = 08/24/16 Pct Recovery = 87% Analysis Date = 08/24/16 Pct Recovery = 87% Analysis Date = 08/19/16 Pct Recovery = 87% Analysis Date = 08/19/16 Pct Recovery = 87% Analysis Date = 08/14/16 Pct Recovery = 88% Analysis Date = 08/14/16 Pct Recovery = 88% Analysis Date = 08/09/16 Pct Recovery = 88% Analysis Date = 08/09/16 Pct Recovery = 88% Analysis Date = 08/05/16 Pct Recovery = 88% Analysis Date = 08/05/16 Pct Recovery = 88% Analysis Date = 07/31/16 Pct Recovery = 88% Analysis Date = 07/31/16 Pct Recovery = 88% Analysis Date = 07/26/16 Pct Recovery = 88% Analysis Date = 07/26/16 Pct Recovery = 88% Analysis Date = 07/21/16 Pct Recovery = 88% Analysis Date = 07/21/16 Pct Recovery = 88% Analysis Date = 07/17/16 Pct Recovery = 88% Analysis Date = 07/17/16 Pct Recovery = 88% Analysis Date = 07/12/16 Pct Recovery = 88% Analysis Date = 07/12/16 Pct Recovery = 88% Analysis Date = 07/07/16 Pct Recovery = 88% Analysis Date = 07/07/16 Pct Recovery = 88% Analysis Date = 07/02/16 Pct Recovery = 88% Analysis Date = 07/02/16 Pct Recovery = 88% Analysis Date = 06/28/16 Pct Recovery = 88% Analysis Date = 06/28/16 Pct Recovery = 88% Analysis Date = 06/23/16 Pct Recovery = 88% Analysis Date = 06/23/16 Pct Recovery = 88% Analysis Date = 06/18/16 Pct Recovery = 88% Analysis Date = 06/18/16 Pct Recovery = 88% Analysis Date = 06/13/16 Pct Recovery = 89% Analysis Date = 06/13/16 Pct Recovery = 89% Analysis Date = 06/08/16 Pct Recovery = 89% Analysis Date = 06/08/16 Pct Recovery = 89% Analysis Date = 06/04/16 Pct Recovery = 89% Analysis Date = 06/04/16 Pct Recovery = 89% Analysis Date = 05/30/16 Pct Recovery = 89% Analysis Date = 05/30/16 Pct Recovery = 89% Analysis Date = 05/25/16 Pct Recovery = 89% Analysis Date = 05/25/16 Pct Recovery = 89% Analysis Date = 05/20/16 Pct Recovery = 89% Analysis Date = 05/20/16 Pct Recovery = 89% Analysis Date = 05/16/16 Pct Recovery = 89% Analysis Date = 05/16/16 Pct Recovery = 89% Analysis Date = 05/11/16 Pct Recovery = 89% Analysis Date = 05/11/16 Pct Recovery = 89% Analysis Date = 05/06/16 Pct Recovery = 89% Analysis Date = 05/06/16 Pct Recovery = 89% Analysis Date = 05/01/16 Pct Recovery = 89% Analysis Date = 05/01/16 Pct Recovery = 89% Analysis Date = 04/27/16 Pct Recovery = 89% Analysis Date = 04/27/16 Pct Recovery = 89% Analysis Date = 04/22/16 Pct Recovery = 90% Analysis Date = 04/22/16 Pct Recovery = 90% Analysis Date = 04/17/16 Pct Recovery = 90% Analysis Date = 04/17/16 Pct Recovery = 90% Analysis Date = 04/12/16 Pct Recovery = 90% Analysis Date = 04/12/16 Pct Recovery = 90% Analysis Date = 04/07/16 Pct Recovery = 90% Analysis Date = 04/07/16 Pct Recovery = 90% Analysis Date = 04/03/16 Pct Recovery = 90% Analysis Date = 04/03/16 Pct Recovery = 90% Analysis Date = 03/29/16 Pct Recovery = 90% Analysis Date = 03/29/16 Pct Recovery = 90% Analysis Date = 03/24/16 Pct Recovery = 90% Analysis Date = 03/24/16 Pct Recovery = 90% Analysis Date = 03/19/16 Pct Recovery = 90% Analysis Date = 03/19/16 Pct Recovery = 90% Analysis Date = 03/15/16 Pct Recovery = 90% Analysis Date = 03/15/16 Pct Recovery = 90% Analysis Date = 03/10/16 Pct Recovery = 90% Analysis Date = 03/10/16 Pct Recovery = 90% Analysis Date = 03/05/16 Pct Recovery = 90% Analysis Date = 03/05/16 Pct Recovery = 90% Analysis Date = 02/29/16 Pct Recovery = 90% Analysis Date = 02/29/16 Pct Recovery = 90% Analysis Date = 02/25/16 Pct Recovery = 91% Analysis Date = 02/25/16 Pct Recovery = 91% Analysis Date = 02/20/16 Pct Recovery = 91% Analysis Date = 02/20/16 Pct Recovery = 91% Analysis Date = 02/15/16 Pct Recovery = 91% Analysis Date = 02/15/16 Pct Recovery = 91% Analysis Date = 02/10/16 Pct Recovery = 91% Analysis Date = 02/10/16 Pct Recovery = 91% Analysis Date = 02/05/16 Pct Recovery = 91% Analysis Date = 02/05/16 Pct Recovery = 91% Analysis Date = 02/01/16 Pct Recovery = 91% Analysis Date = 02/01/16 Pct Recovery = 91% Analysis Date = 01/27/16 Pct Recovery = 91% Analysis Date = 01/27/16 Pct Recovery = 91% Analysis Date = 01/22/16 Pct Recovery = 91% Analysis Date = 01/22/16 Pct Recovery = 91% Analysis Date = 01/17/16 Pct Recovery = 91% Analysis Date = 01/17/16 Pct Recovery = 91% Analysis Date = 01/13/16 Pct Recovery = 91% Analysis Date = 01/13/16 Pct Recovery = 91% Analysis Date = 01/08/16 Pct Recovery = 91% Analysis Date = 01/08/16 Pct Recovery = 91% Analysis Date = 01/03/16 Pct Recovery = 91% Analysis Date = 01/03/16 Pct Recovery = 91% Analysis Date = 12/29/15 Pct Recovery = 92% Analysis Date = 12/29/15 Pct Recovery = 92% Analysis Date = 12/25/15 Pct Recovery = 92% Analysis Date = 12/25/15 Pct Recovery = 92% Analysis Date = 12/20/15 Pct Recovery = 92% Analysis Date = 12/20/15 Pct Recovery = 92% Analysis Date = 12/15/15 Pct Recovery = 92% Analysis Date = 12/15/15 Pct Recovery = 92% Analysis Date = 12/10/15 Pct Recovery = 92% Analysis Date = 12/10/15 Pct Recovery = 92% Analysis Date = 12/05/15 Pct Recovery = 92% Analysis Date = 12/05/15 Pct Recovery = 92% Analysis Date = 12/01/15 Pct Recovery = 92% Analysis Date = 12/01/15 Pct Recovery = 92% Analysis Date = 11/26/15 Pct Recovery = 92% Analysis Date = 11/26/15 Pct Recovery = 92% Analysis Date = 11/21/15 Pct Recovery = 92% Analysis Date = 11/21/15 Pct Recovery = 92% Analysis Date = 11/16/15 Pct Recovery = 92% Analysis Date = 11/16/15 Pct Recovery = 92% Analysis Date = 11/12/15 Pct Recovery = 92% Analysis Date = 11/12/15 Pct Recovery = 92% Analysis Date = 11/07/15 Pct Recovery = 92% Analysis Date = 11/07/15 Pct Recovery = 92% Analysis Date = 11/02/15 Pct Recovery = 92% Analysis Date = 11/02/15 Pct Recovery = 92% Analysis Date = 10/28/15 Pct Recovery = 92% Analysis Date = 10/28/15 Pct Recovery = 92% Analysis Date = 10/24/15 Pct Recovery = 93% Analysis Date = 10/24/15 Pct Recovery = 93% Analysis Date = 10/19/15 Pct Recovery = 93% Analysis Date = 10/19/15 Pct Recovery = 93% Analysis Date = 10/14/15 Pct Recovery = 93% Analysis Date = 10/14/15 Pct Recovery = 93% Analysis Date = 10/09/15 Pct Recovery = 93% Analysis Date = 10/09/15 Pct Recovery = 93% Analysis Date = 10/04/15 Pct Recovery = 93% Analysis Date = 10/04/15 Pct Recovery = 93% Analysis Date = 09/30/15 Pct Recovery = 93% Analysis Date = 09/30/15 Pct Recovery = 93% Analysis Date = 09/25/15 Pct Recovery = 93% Analysis Date = 09/25/15 Pct Recovery = 93% Analysis Date = 09/20/15 Pct Recovery = 93% Analysis Date = 09/20/15 Pct Recovery = 93% Analysis Date = 09/15/15 Pct Recovery = 93% Analysis Date = 09/15/15 Pct Recovery = 93% Analysis Date = 09/11/15 Pct Recovery = 93% Analysis Date = 09/11/15 Pct Recovery = 93% Analysis Date = 09/06/15 Pct Recovery = 93% Analysis Date = 09/06/15 Pct Recovery = 93% Analysis Date = 09/01/15 Pct Recovery = 93% Analysis Date = 09/01/15 Pct Recovery = 93% Analysis Date = 08/27/15 Pct Recovery = 93% Analysis Date = 08/27/15 Pct Recovery = 93% Analysis Date = 08/23/15 Pct Recovery = 93% Analysis Date = 08/23/15 Pct Recovery = 93% Analysis Date = 08/18/15 Pct Recovery = 93% Analysis Date = 08/18/15 Pct Recovery = 93% Analysis Date = 08/13/15 Pct Recovery = 93% Analysis Date = 08/13/15 Pct Recovery = 93% Analysis Date = 08/08/15 Pct Recovery = 93% Analysis Date = 08/08/15 Pct Recovery = 93% Analysis Date = 08/03/15 Pct Recovery = 93% Analysis Date = 08/03/15 Pct Recovery = 93% Analysis Date = 07/30/15 Pct Recovery = 93% Analysis Date = 07/30/15 Pct Recovery = 93% Analysis Date = 07/25/15 Pct Recovery = 93% Analysis Date = 07/25/15 Pct Recovery = 93% Analysis Date = 07/20/15 Pct Recovery = 93% Analysis Date = 07/20/15 Pct Recovery = 93% Analysis Date = 07/15/15 Pct Recovery = 93% Analysis Date = 07/15/15 Pct Recovery = 93% Analysis Date = 07/11/15 Pct Recovery = 93% Analysis Date = 07/11/15 Pct Recovery = 93% Analysis Date = 07/06/15 Pct Recovery = 93% Analysis Date = 07/06/15 Pct Recovery = 93% Analysis Date = 07/01/15 Pct Recovery = 93% Analysis Date = 07/01/15 Pct Recovery = 93% Analysis Date = 06/26/15 Pct Recovery = 93% Analysis Date = 06/26/15 Pct Recovery = 93% Analysis Date = 06/21/15 Pct Recovery = 93% Analysis Date = 06/21/15 Pct Recovery = 93% Analysis Date = 06/17/15 Pct Recovery = 93% Analysis Date = 06/17/15 Pct Recovery = 93% Analysis Date = 06/12/15 Pct Recovery = 93% Analysis Date = 06/12/15 Pct Recovery = 93% Analysis Date = 06/07/15 Pct Recovery = 93% Analysis Date = 06/07/15 Pct Recovery = 93% Analysis Date = 06/02/15 Pct Recovery = 93% Analysis Date = 06/02/15 Pct Recovery = 93% Analysis Date = 05/29/15 Pct Recovery = 93% Analysis Date = 05/29/15 Pct Recovery = 93% Analysis Date = 05/24/15 Pct Recovery = 93% Analysis Date = 05/24/15 Pct Recovery = 93% Analysis Date = 05/19/15 Pct Recovery = 93% Analysis Date = 05/19/15 Pct Recovery = 93% Analysis Date = 05/14/15 Pct Recovery = 93% Analysis Date = 05/14/15 Pct Recovery = 93% Analysis Date = 05/10/15 Pct Recovery = 93% Analysis Date = 05/10/15 Pct Recovery = 93% Analysis Date = 05/05/15 Pct Recovery = 93% Analysis Date = 05/05/15 Pct Recovery = 93% Analysis Date = 04/30/15 Pct Recovery = 93% Analysis Date = 04/30/15 Pct Recovery = 93% Analysis Date = 04/25/15 Pct Recovery = 93% Analysis Date = 04/25/15 Pct Recovery = 93% Analysis Date = 04/20/15 Pct Recovery = 93% Analysis Date = 04/20/15 Pct Recovery = 93% Analysis Date = 04/16/15 Pct Recovery = 93% Analysis Date = 04/16/15 Pct Recovery = 93% Analysis Date = 04/11/15 Pct Recovery = 93% Analysis Date = 04/11/15 Pct Recovery = 93% Analysis Date = 04/06/15 Pct Recovery = 93% Analysis Date = 04/06/15 Pct Recovery = 93% Analysis Date = 04/01/15 Pct Recovery = 93% Analysis Date = 04/01/15 Pct Recovery = 93% Analysis Date = 03/28/15 Pct Recovery = 93% Analysis Date = 03/28/15 Pct Recovery = 93% Analysis Date = 03/23/15 Pct Recovery = 93% Analysis Date = 03/23/15 Pct Recovery = 93% Analysis Date = 03/18/15 Pct Recovery = 93% Analysis Date = 03/18/15 Pct Recovery = 93% Analysis Date = 03/13/15 Pct Recovery = 93% Analysis Date = 03/13/15 Pct Recovery = 93% Analysis Date = 03/09/15 Pct Recovery = 93% Analysis Date = 03/09/15 Pct Recovery = 93% Analysis Date = 03/04/15 Pct Recovery = 93% Analysis Date = 03/04/15 Pct Recovery = 93% Analysis Date = 02/27/15 Pct Recovery = 93% Analysis Date = 02/27/15 Pct Recovery = 93% Analysis Date = 02/22/15 Pct Recovery = 93% Analysis Date = 02/22/15 Pct Recovery = 93% Analysis Date = 02/17/15 Pct Recovery = 93% Analysis Date = 02/17/15 Pct Recovery = 93% Analysis Date = 02/13/15 Pct Recovery = 93% Analysis Date = 02/13/15 Pct Recovery = 93% Analysis Date = 02/08/15 Pct Recovery = 93% Analysis Date = 02/08/15 Pct Recovery = 93% Analysis Date = 02/03/15 Pct Recovery = 93% Analysis Date = 02/03/15 Pct Recovery = 93% Analysis Date = 01/29/15 Pct Recovery = 93% Analysis Date = 01/29/15 Pct Recovery = 93% Analysis Date = 01/25/15 Pct Recovery = 93% Analysis Date = 01/25/15 Pct Recovery = 93% Analysis Date = 01/20/15 Pct Recovery = 93% Analysis Date = 01/20/15 Pct Recovery = 93% Analysis Date = 01/15/15 Pct Recovery = 93% Analysis Date = 01/15/15 Pct Recovery = 93% Analysis Date = 01/10/15 Pct Recovery = 93% Analysis Date = 01/10/15 Pct Recovery = 93% Analysis Date = 01/06/15 Pct Recovery = 93% Analysis Date = 01/06/15 Pct Recovery = 93% Analysis Date = 01/01/15 Pct Recovery = 93% Analysis Date = 01/01/15 Pct Recovery = 93% Analysis Date = 12/27/14 Pct Recovery = 93% Analysis Date = 12/27/14 Pct Recovery = 93% Analysis Date = 12/22/14 Pct Recovery = 93% Analysis Date = 12/22/14 Pct Recovery = 93% Analysis Date = 12/17/14 Pct Recovery = 93% Analysis Date = 12/17/14 Pct Recovery = 93% Analysis Date = 12/13/14 Pct Recovery = 93% Analysis Date = 12/13/14 Pct Recovery = 93% Analysis Date = 12/08/14 Pct Recovery = 93% Analysis Date = 12/08/14 Pct Recovery = 93% Analysis Date = 12/03/14 Pct Recovery = 93% Analysis Date = 12/03/14 Pct Recovery = 93% Analysis Date = 11/28/14 Pct Recovery = 93% Analysis Date = 11/28/14 Pct Recovery = 93% Analysis Date = 11/24/14 Pct Recovery = 93% Analysis Date = 11/24/14 Pct Recovery = 93% Analysis Date = 11/19/14 Pct Recovery = 93% Analysis Date = 11/19/14 Pct Recovery = 93% Analysis Date = 11/14/14 Pct Recovery = 93% Analysis Date = 11/14/14 Pct Recovery = 93% Analysis Date = 11/09/14 Pct Recovery = 93% Analysis Date = 11/09/14 Pct Recovery = 93% Analysis Date = 11/05/14 Pct Recovery = 93% Analysis Date = 11/05/14 Pct Recovery = 93% Analysis Date = 10/31/14 Pct Recovery = 93% Analysis Date = 10/31/14 Pct Recovery = 93% Analysis Date = 10/26/14 Pct Recovery = 93% Analysis Date = 10/26/14 Pct Recovery = 93% Analysis Date = 10/21/14 Pct Recovery = 93% Analysis Date = 10/21/14 Pct Recovery = 93% Analysis Date = 10/16/14 Pct Recovery = 93% Analysis Date = 10/16/14 Pct Recovery = 93% Analysis Date = 10/12/14 Pct Recovery = 93% Analysis Date = 10/12/14 Pct Recovery = 93% Analysis Date = 10/07/14 Pct Recovery = 92% Analysis Date = 10/07/14 Pct Recovery = 92% Analysis Date = 10/02/14 Pct Recovery = 92% Analysis Date = 10/02/14 Pct Recovery = 92% Analysis Date = 09/27/14 Pct Recovery = 92% Analysis Date = 09/27/14 Pct Recovery = 92% Analysis Date = 09/23/14 Pct Recovery = 92% Analysis Date = 09/23/14 Pct Recovery = 92% Analysis Date = 09/18/14 Pct Recovery = 92% Analysis Date = 09/18/14 Pct Recovery = 92% Analysis Date = 09/13/14 Pct Recovery = 92% Analysis Date = 09/13/14 Pct Recovery = 92% Analysis Date = 09/08/14 Pct Recovery = 92% Analysis Date = 09/08/14 Pct Recovery = 92% Analysis Date = 09/04/14 Pct Recovery = 92% Analysis Date = 09/04/14 Pct Recovery = 92% Analysis Date = 08/30/14 Pct Recovery = 92% Analysis Date = 08/30/14 Pct Recovery = 92% Analysis Date = 08/25/14 Pct Recovery = 92% Analysis Date = 08/25/14 Pct Recovery = 92% Analysis Date = 08/20/14 Pct Recovery = 92% Analysis Date = 08/20/14 Pct Recovery = 92% Analysis Date = 08/15/14 Pct Recovery = 92% Analysis Date = 08/15/14 Pct Recovery = 92% Analysis Date = 08/11/14 Pct Recovery = 92% Analysis Date = 08/11/14 Pct Recovery = 92% Analysis Date = 08/06/14 Pct Recovery = 92% Analysis Date = 08/06/14 Pct Recovery = 92% Analysis Date = 08/01/14 Pct Recovery = 92% Analysis Date = 08/01/14 Pct Recovery = 92% Analysis Date = 07/27/14 Pct Recovery = 92% Analysis Date = 07/27/14 Pct Recovery = 92% Analysis Date = 07/23/14 Pct Recovery = 91% Analysis Date = 07/23/14 Pct Recovery = 91% Analysis Date = 07/18/14 Pct Recovery = 91% Analysis Date = 07/18/14 Pct Recovery = 91% Analysis Date = 07/13/14 Pct Recovery = 91% Analysis Date = 07/13/14 Pct Recovery = 91% Analysis Date = 07/08/14 Pct Recovery = 91% Analysis Date = 07/08/14 Pct Recovery = 91% Analysis Date = 07/04/14 Pct Recovery = 91% Analysis Date = 07/04/14 Pct Recovery = 91% Analysis Date = 06/29/14 Pct Recovery = 91% Analysis Date = 06/29/14 Pct Recovery = 91% Analysis Date = 06/24/14 Pct Recovery = 91% Analysis Date = 06/24/14 Pct Recovery = 91% Analysis Date = 06/19/14 Pct Recovery = 91% Analysis Date = 06/19/14 Pct Recovery = 91% Analysis Date = 06/14/14 Pct Recovery = 91% Analysis Date = 06/14/14 Pct Recovery = 91% Analysis Date = 06/10/14 Pct Recovery = 91% Analysis Date = 06/10/14 Pct Recovery = 91% Analysis Date = 06/05/14 Pct Recovery = 91% Analysis Date = 06/05/14 Pct Recovery = 91% Analysis Date = 05/31/14 Pct Recovery = 91% Analysis Date = 05/31/14 Pct Recovery = 91% Analysis Date = 05/26/14 Pct Recovery = 90% Analysis Date = 05/26/14 Pct Recovery = 90% Analysis Date = 05/22/14 Pct Recovery = 90% Analysis Date = 05/22/14 Pct Recovery = 90% Analysis Date = 05/17/14 Pct Recovery = 90% Analysis Date = 05/17/14 Pct Recovery = 90% Analysis Date = 05/12/14 Pct Recovery = 90% Analysis Date = 05/12/14 Pct Recovery = 90% Analysis Date = 05/07/14 Pct Recovery = 90% Analysis Date = 05/07/14 Pct Recovery = 90% Analysis Date = 05/03/14 Pct Recovery = 90% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
1,2,3-TRICHLOROBENZENE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 42 91% 8% 91% 8%
Total 42 91% 8% 91% 8%

Sample Statistics
1,2,3-TRICHLOROBENZENE

Characteristic N % % Basis
Plotted 42 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 42 .  
False Negatives 0 0% 0 out of 42
Not Spiked 24 .  
False Positives 0 0% 0 out of 24

BQS OBSP Determination:
1,2,3-TRICHLOROPROPANE
METHOD: 4440 , TESTIDCODE: 77443GCM66
Open Data Set

Analysis Date = 12/16/16 SpikeMix = NSI 041816AVOC: 40 µl & ChemService 5082900: 40 µl Pct Recovery = 94% Analysis Date = 12/12/16 SpikeMix = Accu 216041125: 40 µl & Crescent 03FF058: 40 µl Pct Recovery = 98% Analysis Date = 08/04/16 SpikeMix = Crescent 03FF058: 40 µl & Supelco LC20141V: 40 µl Pct Recovery = 94% Analysis Date = 07/14/16 SpikeMix = Accu 216041125: 40 µl & NSI 041816AVOC: 40 µl Pct Recovery = 114% Analysis Date = 11/21/16 SpikeMix = Crescent 03FF058: 25 µl & Supelco LC20141V: 25 µl Pct Recovery = 91% Analysis Date = 08/26/16 SpikeMix = NSI 041816AVOC: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 100% Analysis Date = 06/30/16 SpikeMix = Crescent 03FF058: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 97% Analysis Date = 06/21/16 SpikeMix = Phenova B20160319: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 100% Analysis Date = 05/24/16 SpikeMix = Accu 216041125: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 96% Analysis Date = 03/19/15 SpikeMix = Spex Organics C1140417015: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 111% Analysis Date = 12/17/14 SpikeMix = Supelco LC06438: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 92% Analysis Date = 11/14/14 SpikeMix = Crescent 03DD004: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 85% Analysis Date = 06/10/14 SpikeMix = Crescent 03DD004: 20 µl & NSI 032614: 20 µl Pct Recovery = 85% Analysis Date = 04/09/15 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 91% Analysis Date = 08/19/14 SpikeMix = Spex Organics C1140417015: 20 µl & Accu 214031115: 20 µl Pct Recovery = 87% Analysis Date = 07/01/14 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 99% Analysis Date = 05/01/14 SpikeMix = Accu 214031115: 20 µl & NSI 032614: 20 µl Pct Recovery = 88% Analysis Date = 08/15/15 SpikeMix = Supelco LC13545: 25 µl & Crescent 04EE008: 25 µl Pct Recovery = 104% Analysis Date = 06/16/15 SpikeMix = ERA 0406-15-03: 25 µl & Supelco LC13545: 25 µl Pct Recovery = 86% Analysis Date = 10/13/16 SpikeMix = Accu 216041125: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 108% Analysis Date = 10/13/16 SpikeMix = NSI 041816AVOC: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 85% Analysis Date = 09/28/16 SpikeMix = Crescent 03FF058: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 90% Analysis Date = 09/08/16 SpikeMix = Phenova B20160319: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 94% Analysis Date = 08/20/16 SpikeMix = Accu 216041125: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 98% Analysis Date = 07/29/16 SpikeMix = Phenova B20160319: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 113% Analysis Date = 06/10/16 SpikeMix = NSI 041816AVOC: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 96% Analysis Date = 04/26/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 116% Analysis Date = 04/02/16 SpikeMix = Supelco LC13545: 15 µl & Accu 215041380: 15 µl Pct Recovery = 104% Analysis Date = 02/05/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 81% Analysis Date = 12/18/15 SpikeMix = Supelco LC13545: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 101% Analysis Date = 11/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 84% Analysis Date = 10/16/15 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 93% Analysis Date = 05/09/15 SpikeMix = Spex Organics EN150428007: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 95% Analysis Date = 11/06/14 SpikeMix = Spex Organics C1140417015: 10 µl & Crescent 03DD004: 10 µl Pct Recovery = 99% Analysis Date = 10/04/14 SpikeMix = Crescent 03DD004: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 96% Analysis Date = 07/29/14 SpikeMix = Crescent 03DD004: 10 µl & NSI 032614: 10 µl Pct Recovery = 89% Analysis Date = 05/03/14 SpikeMix = Crescent 03DD004: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 99% Analysis Date = 01/13/15 SpikeMix = Accu 214031115: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 75% Analysis Date = 09/09/14 SpikeMix = Accu 214031115: 10 µl & NSI 032614: 10 µl Pct Recovery = 107% Analysis Date = 07/23/14 SpikeMix = Spex Organics C1140417015: 10 µl & Accu 214031115: 10 µl Pct Recovery = 103% Analysis Date = 06/18/14 SpikeMix = Supelco LC06438: 10 µl & Accu 214031115: 10 µl Pct Recovery = 103% Analysis Date = 05/13/16 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 103% Analysis Date = 03/17/16 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 94% Analysis Date = 02/18/16 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 108% Analysis Date = 12/10/15 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 96% Analysis Date = 11/12/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 82% Analysis Date = 09/03/15 SpikeMix = NSI 050515AVOC: 10 µl & Spex Organics EN150428007: 10 µl Pct Recovery = 100% Analysis Date = 06/27/15 SpikeMix = ERA 0406-15-03: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 100% Analysis Date = 05/21/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 96% Analysis Date = 05/09/15 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 101% Analysis Date = 12/15/16 Pct Recovery = 97% Analysis Date = 12/11/16 Pct Recovery = 97% Analysis Date = 12/11/16 Pct Recovery = 97% Analysis Date = 12/06/16 Pct Recovery = 97% Analysis Date = 12/06/16 Pct Recovery = 97% Analysis Date = 12/01/16 Pct Recovery = 97% Analysis Date = 12/01/16 Pct Recovery = 97% Analysis Date = 11/26/16 Pct Recovery = 97% Analysis Date = 11/26/16 Pct Recovery = 97% Analysis Date = 11/21/16 Pct Recovery = 98% Analysis Date = 11/21/16 Pct Recovery = 98% Analysis Date = 11/17/16 Pct Recovery = 98% Analysis Date = 11/17/16 Pct Recovery = 98% Analysis Date = 11/12/16 Pct Recovery = 98% Analysis Date = 11/12/16 Pct Recovery = 98% Analysis Date = 11/07/16 Pct Recovery = 98% Analysis Date = 11/07/16 Pct Recovery = 98% Analysis Date = 11/02/16 Pct Recovery = 98% Analysis Date = 11/02/16 Pct Recovery = 98% Analysis Date = 10/28/16 Pct Recovery = 98% Analysis Date = 10/28/16 Pct Recovery = 98% Analysis Date = 10/24/16 Pct Recovery = 98% Analysis Date = 10/24/16 Pct Recovery = 98% Analysis Date = 10/19/16 Pct Recovery = 98% Analysis Date = 10/19/16 Pct Recovery = 98% Analysis Date = 10/14/16 Pct Recovery = 98% Analysis Date = 10/14/16 Pct Recovery = 98% Analysis Date = 10/09/16 Pct Recovery = 98% Analysis Date = 10/09/16 Pct Recovery = 98% Analysis Date = 10/04/16 Pct Recovery = 98% Analysis Date = 10/04/16 Pct Recovery = 98% Analysis Date = 09/30/16 Pct Recovery = 98% Analysis Date = 09/30/16 Pct Recovery = 98% Analysis Date = 09/25/16 Pct Recovery = 98% Analysis Date = 09/25/16 Pct Recovery = 98% Analysis Date = 09/20/16 Pct Recovery = 98% Analysis Date = 09/20/16 Pct Recovery = 98% Analysis Date = 09/15/16 Pct Recovery = 98% Analysis Date = 09/15/16 Pct Recovery = 98% Analysis Date = 09/10/16 Pct Recovery = 98% Analysis Date = 09/10/16 Pct Recovery = 98% Analysis Date = 09/06/16 Pct Recovery = 98% Analysis Date = 09/06/16 Pct Recovery = 98% Analysis Date = 09/01/16 Pct Recovery = 98% Analysis Date = 09/01/16 Pct Recovery = 98% Analysis Date = 08/27/16 Pct Recovery = 98% Analysis Date = 08/27/16 Pct Recovery = 98% Analysis Date = 08/22/16 Pct Recovery = 98% Analysis Date = 08/22/16 Pct Recovery = 98% Analysis Date = 08/17/16 Pct Recovery = 98% Analysis Date = 08/17/16 Pct Recovery = 98% Analysis Date = 08/13/16 Pct Recovery = 98% Analysis Date = 08/13/16 Pct Recovery = 98% Analysis Date = 08/08/16 Pct Recovery = 98% Analysis Date = 08/08/16 Pct Recovery = 98% Analysis Date = 08/03/16 Pct Recovery = 98% Analysis Date = 08/03/16 Pct Recovery = 98% Analysis Date = 07/29/16 Pct Recovery = 98% Analysis Date = 07/29/16 Pct Recovery = 98% Analysis Date = 07/24/16 Pct Recovery = 98% Analysis Date = 07/24/16 Pct Recovery = 98% Analysis Date = 07/20/16 Pct Recovery = 98% Analysis Date = 07/20/16 Pct Recovery = 98% Analysis Date = 07/15/16 Pct Recovery = 98% Analysis Date = 07/15/16 Pct Recovery = 98% Analysis Date = 07/10/16 Pct Recovery = 98% Analysis Date = 07/10/16 Pct Recovery = 98% Analysis Date = 07/05/16 Pct Recovery = 98% Analysis Date = 07/05/16 Pct Recovery = 98% Analysis Date = 06/30/16 Pct Recovery = 98% Analysis Date = 06/30/16 Pct Recovery = 98% Analysis Date = 06/26/16 Pct Recovery = 98% Analysis Date = 06/26/16 Pct Recovery = 98% Analysis Date = 06/21/16 Pct Recovery = 98% Analysis Date = 06/21/16 Pct Recovery = 98% Analysis Date = 06/16/16 Pct Recovery = 98% Analysis Date = 06/16/16 Pct Recovery = 98% Analysis Date = 06/11/16 Pct Recovery = 98% Analysis Date = 06/11/16 Pct Recovery = 98% Analysis Date = 06/06/16 Pct Recovery = 98% Analysis Date = 06/06/16 Pct Recovery = 98% Analysis Date = 06/02/16 Pct Recovery = 98% Analysis Date = 06/02/16 Pct Recovery = 98% Analysis Date = 05/28/16 Pct Recovery = 98% Analysis Date = 05/28/16 Pct Recovery = 98% Analysis Date = 05/23/16 Pct Recovery = 98% Analysis Date = 05/23/16 Pct Recovery = 98% Analysis Date = 05/18/16 Pct Recovery = 98% Analysis Date = 05/18/16 Pct Recovery = 98% Analysis Date = 05/13/16 Pct Recovery = 98% Analysis Date = 05/13/16 Pct Recovery = 98% Analysis Date = 05/09/16 Pct Recovery = 98% Analysis Date = 05/09/16 Pct Recovery = 98% Analysis Date = 05/04/16 Pct Recovery = 98% Analysis Date = 05/04/16 Pct Recovery = 98% Analysis Date = 04/29/16 Pct Recovery = 98% Analysis Date = 04/29/16 Pct Recovery = 98% Analysis Date = 04/24/16 Pct Recovery = 98% Analysis Date = 04/24/16 Pct Recovery = 98% Analysis Date = 04/19/16 Pct Recovery = 98% Analysis Date = 04/19/16 Pct Recovery = 98% Analysis Date = 04/15/16 Pct Recovery = 98% Analysis Date = 04/15/16 Pct Recovery = 98% Analysis Date = 04/10/16 Pct Recovery = 98% Analysis Date = 04/10/16 Pct Recovery = 98% Analysis Date = 04/05/16 Pct Recovery = 98% Analysis Date = 04/05/16 Pct Recovery = 98% Analysis Date = 03/31/16 Pct Recovery = 98% Analysis Date = 03/31/16 Pct Recovery = 98% Analysis Date = 03/26/16 Pct Recovery = 98% Analysis Date = 03/26/16 Pct Recovery = 98% Analysis Date = 03/22/16 Pct Recovery = 98% Analysis Date = 03/22/16 Pct Recovery = 98% Analysis Date = 03/17/16 Pct Recovery = 98% Analysis Date = 03/17/16 Pct Recovery = 98% Analysis Date = 03/12/16 Pct Recovery = 98% Analysis Date = 03/12/16 Pct Recovery = 98% Analysis Date = 03/07/16 Pct Recovery = 98% Analysis Date = 03/07/16 Pct Recovery = 98% Analysis Date = 03/02/16 Pct Recovery = 98% Analysis Date = 03/02/16 Pct Recovery = 98% Analysis Date = 02/27/16 Pct Recovery = 97% Analysis Date = 02/27/16 Pct Recovery = 97% Analysis Date = 02/22/16 Pct Recovery = 97% Analysis Date = 02/22/16 Pct Recovery = 97% Analysis Date = 02/17/16 Pct Recovery = 97% Analysis Date = 02/17/16 Pct Recovery = 97% Analysis Date = 02/12/16 Pct Recovery = 97% Analysis Date = 02/12/16 Pct Recovery = 97% Analysis Date = 02/07/16 Pct Recovery = 97% Analysis Date = 02/07/16 Pct Recovery = 97% Analysis Date = 02/03/16 Pct Recovery = 97% Analysis Date = 02/03/16 Pct Recovery = 97% Analysis Date = 01/29/16 Pct Recovery = 97% Analysis Date = 01/29/16 Pct Recovery = 97% Analysis Date = 01/24/16 Pct Recovery = 97% Analysis Date = 01/24/16 Pct Recovery = 97% Analysis Date = 01/19/16 Pct Recovery = 97% Analysis Date = 01/19/16 Pct Recovery = 97% Analysis Date = 01/14/16 Pct Recovery = 97% Analysis Date = 01/14/16 Pct Recovery = 97% Analysis Date = 01/10/16 Pct Recovery = 97% Analysis Date = 01/10/16 Pct Recovery = 97% Analysis Date = 01/05/16 Pct Recovery = 97% Analysis Date = 01/05/16 Pct Recovery = 97% Analysis Date = 12/31/15 Pct Recovery = 97% Analysis Date = 12/31/15 Pct Recovery = 97% Analysis Date = 12/26/15 Pct Recovery = 97% Analysis Date = 12/26/15 Pct Recovery = 97% Analysis Date = 12/21/15 Pct Recovery = 97% Analysis Date = 12/21/15 Pct Recovery = 97% Analysis Date = 12/17/15 Pct Recovery = 96% Analysis Date = 12/17/15 Pct Recovery = 96% Analysis Date = 12/12/15 Pct Recovery = 96% Analysis Date = 12/12/15 Pct Recovery = 96% Analysis Date = 12/07/15 Pct Recovery = 96% Analysis Date = 12/07/15 Pct Recovery = 96% Analysis Date = 12/02/15 Pct Recovery = 96% Analysis Date = 12/02/15 Pct Recovery = 96% Analysis Date = 11/27/15 Pct Recovery = 96% Analysis Date = 11/27/15 Pct Recovery = 96% Analysis Date = 11/23/15 Pct Recovery = 96% Analysis Date = 11/23/15 Pct Recovery = 96% Analysis Date = 11/18/15 Pct Recovery = 96% Analysis Date = 11/18/15 Pct Recovery = 96% Analysis Date = 11/13/15 Pct Recovery = 96% Analysis Date = 11/13/15 Pct Recovery = 96% Analysis Date = 11/08/15 Pct Recovery = 96% Analysis Date = 11/08/15 Pct Recovery = 96% Analysis Date = 11/03/15 Pct Recovery = 96% Analysis Date = 11/03/15 Pct Recovery = 96% Analysis Date = 10/30/15 Pct Recovery = 96% Analysis Date = 10/30/15 Pct Recovery = 96% Analysis Date = 10/25/15 Pct Recovery = 96% Analysis Date = 10/25/15 Pct Recovery = 96% Analysis Date = 10/20/15 Pct Recovery = 96% Analysis Date = 10/20/15 Pct Recovery = 96% Analysis Date = 10/15/15 Pct Recovery = 96% Analysis Date = 10/15/15 Pct Recovery = 96% Analysis Date = 10/10/15 Pct Recovery = 96% Analysis Date = 10/10/15 Pct Recovery = 96% Analysis Date = 10/06/15 Pct Recovery = 96% Analysis Date = 10/06/15 Pct Recovery = 96% Analysis Date = 10/01/15 Pct Recovery = 96% Analysis Date = 10/01/15 Pct Recovery = 96% Analysis Date = 09/26/15 Pct Recovery = 96% Analysis Date = 09/26/15 Pct Recovery = 96% Analysis Date = 09/21/15 Pct Recovery = 96% Analysis Date = 09/21/15 Pct Recovery = 96% Analysis Date = 09/16/15 Pct Recovery = 96% Analysis Date = 09/16/15 Pct Recovery = 96% Analysis Date = 09/12/15 Pct Recovery = 96% Analysis Date = 09/12/15 Pct Recovery = 96% Analysis Date = 09/07/15 Pct Recovery = 95% Analysis Date = 09/07/15 Pct Recovery = 95% Analysis Date = 09/02/15 Pct Recovery = 95% Analysis Date = 09/02/15 Pct Recovery = 95% Analysis Date = 08/28/15 Pct Recovery = 95% Analysis Date = 08/28/15 Pct Recovery = 95% Analysis Date = 08/23/15 Pct Recovery = 95% Analysis Date = 08/23/15 Pct Recovery = 95% Analysis Date = 08/19/15 Pct Recovery = 95% Analysis Date = 08/19/15 Pct Recovery = 95% Analysis Date = 08/14/15 Pct Recovery = 95% Analysis Date = 08/14/15 Pct Recovery = 95% Analysis Date = 08/09/15 Pct Recovery = 95% Analysis Date = 08/09/15 Pct Recovery = 95% Analysis Date = 08/04/15 Pct Recovery = 95% Analysis Date = 08/04/15 Pct Recovery = 95% Analysis Date = 07/30/15 Pct Recovery = 95% Analysis Date = 07/30/15 Pct Recovery = 95% Analysis Date = 07/26/15 Pct Recovery = 95% Analysis Date = 07/26/15 Pct Recovery = 95% Analysis Date = 07/21/15 Pct Recovery = 95% Analysis Date = 07/21/15 Pct Recovery = 95% Analysis Date = 07/16/15 Pct Recovery = 95% Analysis Date = 07/16/15 Pct Recovery = 95% Analysis Date = 07/11/15 Pct Recovery = 95% Analysis Date = 07/11/15 Pct Recovery = 95% Analysis Date = 07/06/15 Pct Recovery = 95% Analysis Date = 07/06/15 Pct Recovery = 95% Analysis Date = 07/02/15 Pct Recovery = 95% Analysis Date = 07/02/15 Pct Recovery = 95% Analysis Date = 06/27/15 Pct Recovery = 95% Analysis Date = 06/27/15 Pct Recovery = 95% Analysis Date = 06/22/15 Pct Recovery = 95% Analysis Date = 06/22/15 Pct Recovery = 95% Analysis Date = 06/17/15 Pct Recovery = 95% Analysis Date = 06/17/15 Pct Recovery = 95% Analysis Date = 06/12/15 Pct Recovery = 95% Analysis Date = 06/12/15 Pct Recovery = 95% Analysis Date = 06/08/15 Pct Recovery = 95% Analysis Date = 06/08/15 Pct Recovery = 95% Analysis Date = 06/03/15 Pct Recovery = 95% Analysis Date = 06/03/15 Pct Recovery = 95% Analysis Date = 05/29/15 Pct Recovery = 95% Analysis Date = 05/29/15 Pct Recovery = 95% Analysis Date = 05/24/15 Pct Recovery = 95% Analysis Date = 05/24/15 Pct Recovery = 95% Analysis Date = 05/19/15 Pct Recovery = 94% Analysis Date = 05/19/15 Pct Recovery = 94% Analysis Date = 05/15/15 Pct Recovery = 94% Analysis Date = 05/15/15 Pct Recovery = 94% Analysis Date = 05/10/15 Pct Recovery = 94% Analysis Date = 05/10/15 Pct Recovery = 94% Analysis Date = 05/05/15 Pct Recovery = 95% Analysis Date = 05/05/15 Pct Recovery = 95% Analysis Date = 04/30/15 Pct Recovery = 95% Analysis Date = 04/30/15 Pct Recovery = 95% Analysis Date = 04/25/15 Pct Recovery = 95% Analysis Date = 04/25/15 Pct Recovery = 95% Analysis Date = 04/21/15 Pct Recovery = 95% Analysis Date = 04/21/15 Pct Recovery = 95% Analysis Date = 04/16/15 Pct Recovery = 95% Analysis Date = 04/16/15 Pct Recovery = 95% Analysis Date = 04/11/15 Pct Recovery = 95% Analysis Date = 04/11/15 Pct Recovery = 95% Analysis Date = 04/06/15 Pct Recovery = 95% Analysis Date = 04/06/15 Pct Recovery = 95% Analysis Date = 04/01/15 Pct Recovery = 95% Analysis Date = 04/01/15 Pct Recovery = 95% Analysis Date = 03/28/15 Pct Recovery = 95% Analysis Date = 03/28/15 Pct Recovery = 95% Analysis Date = 03/23/15 Pct Recovery = 95% Analysis Date = 03/23/15 Pct Recovery = 95% Analysis Date = 03/18/15 Pct Recovery = 95% Analysis Date = 03/18/15 Pct Recovery = 95% Analysis Date = 03/13/15 Pct Recovery = 95% Analysis Date = 03/13/15 Pct Recovery = 95% Analysis Date = 03/08/15 Pct Recovery = 95% Analysis Date = 03/08/15 Pct Recovery = 95% Analysis Date = 03/04/15 Pct Recovery = 95% Analysis Date = 03/04/15 Pct Recovery = 95% Analysis Date = 02/27/15 Pct Recovery = 95% Analysis Date = 02/27/15 Pct Recovery = 95% Analysis Date = 02/22/15 Pct Recovery = 95% Analysis Date = 02/22/15 Pct Recovery = 95% Analysis Date = 02/17/15 Pct Recovery = 95% Analysis Date = 02/17/15 Pct Recovery = 95% Analysis Date = 02/12/15 Pct Recovery = 95% Analysis Date = 02/12/15 Pct Recovery = 95% Analysis Date = 02/08/15 Pct Recovery = 95% Analysis Date = 02/08/15 Pct Recovery = 95% Analysis Date = 02/03/15 Pct Recovery = 95% Analysis Date = 02/03/15 Pct Recovery = 95% Analysis Date = 01/29/15 Pct Recovery = 95% Analysis Date = 01/29/15 Pct Recovery = 95% Analysis Date = 01/24/15 Pct Recovery = 95% Analysis Date = 01/24/15 Pct Recovery = 95% Analysis Date = 01/19/15 Pct Recovery = 95% Analysis Date = 01/19/15 Pct Recovery = 95% Analysis Date = 01/15/15 Pct Recovery = 95% Analysis Date = 01/15/15 Pct Recovery = 95% Analysis Date = 01/10/15 Pct Recovery = 95% Analysis Date = 01/10/15 Pct Recovery = 95% Analysis Date = 01/05/15 Pct Recovery = 95% Analysis Date = 01/05/15 Pct Recovery = 95% Analysis Date = 12/31/14 Pct Recovery = 95% Analysis Date = 12/31/14 Pct Recovery = 95% Analysis Date = 12/26/14 Pct Recovery = 95% Analysis Date = 12/26/14 Pct Recovery = 95% Analysis Date = 12/22/14 Pct Recovery = 95% Analysis Date = 12/22/14 Pct Recovery = 95% Analysis Date = 12/17/14 Pct Recovery = 95% Analysis Date = 12/17/14 Pct Recovery = 95% Analysis Date = 12/12/14 Pct Recovery = 95% Analysis Date = 12/12/14 Pct Recovery = 95% Analysis Date = 12/07/14 Pct Recovery = 95% Analysis Date = 12/07/14 Pct Recovery = 95% Analysis Date = 12/02/14 Pct Recovery = 95% Analysis Date = 12/02/14 Pct Recovery = 95% Analysis Date = 11/28/14 Pct Recovery = 95% Analysis Date = 11/28/14 Pct Recovery = 95% Analysis Date = 11/23/14 Pct Recovery = 95% Analysis Date = 11/23/14 Pct Recovery = 95% Analysis Date = 11/18/14 Pct Recovery = 95% Analysis Date = 11/18/14 Pct Recovery = 95% Analysis Date = 11/13/14 Pct Recovery = 95% Analysis Date = 11/13/14 Pct Recovery = 95% Analysis Date = 11/08/14 Pct Recovery = 95% Analysis Date = 11/08/14 Pct Recovery = 95% Analysis Date = 11/04/14 Pct Recovery = 95% Analysis Date = 11/04/14 Pct Recovery = 95% Analysis Date = 10/30/14 Pct Recovery = 95% Analysis Date = 10/30/14 Pct Recovery = 95% Analysis Date = 10/25/14 Pct Recovery = 95% Analysis Date = 10/25/14 Pct Recovery = 95% Analysis Date = 10/20/14 Pct Recovery = 95% Analysis Date = 10/20/14 Pct Recovery = 95% Analysis Date = 10/15/14 Pct Recovery = 95% Analysis Date = 10/15/14 Pct Recovery = 95% Analysis Date = 10/11/14 Pct Recovery = 95% Analysis Date = 10/11/14 Pct Recovery = 95% Analysis Date = 10/06/14 Pct Recovery = 95% Analysis Date = 10/06/14 Pct Recovery = 95% Analysis Date = 10/01/14 Pct Recovery = 95% Analysis Date = 10/01/14 Pct Recovery = 95% Analysis Date = 09/26/14 Pct Recovery = 95% Analysis Date = 09/26/14 Pct Recovery = 95% Analysis Date = 09/21/14 Pct Recovery = 95% Analysis Date = 09/21/14 Pct Recovery = 95% Analysis Date = 09/17/14 Pct Recovery = 95% Analysis Date = 09/17/14 Pct Recovery = 95% Analysis Date = 09/12/14 Pct Recovery = 95% Analysis Date = 09/12/14 Pct Recovery = 95% Analysis Date = 09/07/14 Pct Recovery = 95% Analysis Date = 09/07/14 Pct Recovery = 95% Analysis Date = 09/02/14 Pct Recovery = 95% Analysis Date = 09/02/14 Pct Recovery = 95% Analysis Date = 08/28/14 Pct Recovery = 95% Analysis Date = 08/28/14 Pct Recovery = 95% Analysis Date = 08/24/14 Pct Recovery = 95% Analysis Date = 08/24/14 Pct Recovery = 95% Analysis Date = 08/19/14 Pct Recovery = 95% Analysis Date = 08/19/14 Pct Recovery = 95% Analysis Date = 08/14/14 Pct Recovery = 95% Analysis Date = 08/14/14 Pct Recovery = 95% Analysis Date = 08/09/14 Pct Recovery = 95% Analysis Date = 08/09/14 Pct Recovery = 95% Analysis Date = 08/04/14 Pct Recovery = 95% Analysis Date = 08/04/14 Pct Recovery = 95% Analysis Date = 07/31/14 Pct Recovery = 95% Analysis Date = 07/31/14 Pct Recovery = 95% Analysis Date = 07/26/14 Pct Recovery = 95% Analysis Date = 07/26/14 Pct Recovery = 95% Analysis Date = 07/21/14 Pct Recovery = 95% Analysis Date = 07/21/14 Pct Recovery = 95% Analysis Date = 07/16/14 Pct Recovery = 95% Analysis Date = 07/16/14 Pct Recovery = 95% Analysis Date = 07/11/14 Pct Recovery = 95% Analysis Date = 07/11/14 Pct Recovery = 95% Analysis Date = 07/07/14 Pct Recovery = 95% Analysis Date = 07/07/14 Pct Recovery = 95% Analysis Date = 07/02/14 Pct Recovery = 95% Analysis Date = 07/02/14 Pct Recovery = 95% Analysis Date = 06/27/14 Pct Recovery = 95% Analysis Date = 06/27/14 Pct Recovery = 95% Analysis Date = 06/22/14 Pct Recovery = 95% Analysis Date = 06/22/14 Pct Recovery = 95% Analysis Date = 06/17/14 Pct Recovery = 95% Analysis Date = 06/17/14 Pct Recovery = 95% Analysis Date = 06/13/14 Pct Recovery = 95% Analysis Date = 06/13/14 Pct Recovery = 95% Analysis Date = 06/08/14 Pct Recovery = 95% Analysis Date = 06/08/14 Pct Recovery = 95% Analysis Date = 06/03/14 Pct Recovery = 95% Analysis Date = 06/03/14 Pct Recovery = 95% Analysis Date = 05/29/14 Pct Recovery = 95% Analysis Date = 05/29/14 Pct Recovery = 95% Analysis Date = 05/24/14 Pct Recovery = 95% Analysis Date = 05/24/14 Pct Recovery = 95% Analysis Date = 05/20/14 Pct Recovery = 95% Analysis Date = 05/20/14 Pct Recovery = 95% Analysis Date = 05/15/14 Pct Recovery = 95% Analysis Date = 05/15/14 Pct Recovery = 95% Analysis Date = 05/10/14 Pct Recovery = 95% Analysis Date = 05/10/14 Pct Recovery = 95% Analysis Date = 05/05/14 Pct Recovery = 95% Analysis Date = 05/05/14 Pct Recovery = 95% Analysis Date = 05/01/14 Pct Recovery = 95% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
1,2,3-TRICHLOROPROPANE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 50 96% 9% 96% 7%
Total 50 96% 9% 96% 7%

Sample Statistics
1,2,3-TRICHLOROPROPANE

Characteristic N % % Basis
Plotted 50 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 50 .  
False Negatives 0 0% 0 out of 50
Not Spiked 23 .  
False Positives 0 0% 0 out of 23

BQS OBSP Determination:
1,2,3-TRIMETHYLBENZENE
METHOD: 4440 , TESTIDCODE: 77221GCM66
Open Data Set

Analysis Date = 12/16/16 SpikeMix = NSI 041816AVOC: 40 µl & ChemService 5082900: 40 µl Pct Recovery = 88% Analysis Date = 08/04/16 SpikeMix = Crescent 03FF058: 40 µl & Supelco LC20141V: 40 µl Pct Recovery = 75% Analysis Date = 07/20/16 SpikeMix = Supelco LC20141V: 40 µl & Accu 216041125: 40 µl Pct Recovery = 98% Analysis Date = 11/21/16 SpikeMix = Crescent 03FF058: 25 µl & Supelco LC20141V: 25 µl Pct Recovery = 82% Analysis Date = 09/08/16 SpikeMix = Supelco LC20141V: 25 µl & Accu 216041125: 25 µl Pct Recovery = 84% Analysis Date = 08/26/16 SpikeMix = NSI 041816AVOC: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 77% Analysis Date = 08/12/16 SpikeMix = ChemService 5082900: 25 µl & Phenova B20160319: 25 µl Pct Recovery = 88% Analysis Date = 06/30/16 SpikeMix = Crescent 03FF058: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 77% Analysis Date = 04/09/15 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 79% Analysis Date = 03/06/15 SpikeMix = ERA 0227-14-06.1A: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 92% Analysis Date = 11/14/14 SpikeMix = Crescent 03DD004: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 79% Analysis Date = 08/16/14 SpikeMix = ERA 0227-14-06.1A: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 77% Analysis Date = 07/01/14 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 76% Analysis Date = 11/22/14 SpikeMix = NSI 032614: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 81% Analysis Date = 06/10/14 SpikeMix = Crescent 03DD004: 20 µl & NSI 032614: 20 µl Pct Recovery = 74% Analysis Date = 06/10/14 SpikeMix = NSI 032614: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 83% Analysis Date = 05/01/14 SpikeMix = Accu 214031115: 20 µl & NSI 032614: 20 µl Pct Recovery = 67% Analysis Date = 09/29/15 SpikeMix = Accu 215041380: 25 µl & ERA 0406-15-03: 25 µl Pct Recovery = 84% Analysis Date = 07/13/15 SpikeMix = Crescent 04EE008: 25 µl & NSI 050515AVOC: 25 µl Pct Recovery = 73% Analysis Date = 06/16/15 SpikeMix = ERA 0406-15-03: 25 µl & Supelco LC13545: 25 µl Pct Recovery = 86% Analysis Date = 11/29/16 SpikeMix = ChemService 5082900: 15 µl & Phenova B20160319: 15 µl Pct Recovery = 92% Analysis Date = 10/13/16 SpikeMix = NSI 041816AVOC: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 68% Analysis Date = 09/28/16 SpikeMix = Crescent 03FF058: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 75% Analysis Date = 06/30/16 SpikeMix = ChemService 5082900: 15 µl & Accu 216041125: 15 µl Pct Recovery = 78% Analysis Date = 06/10/16 SpikeMix = NSI 041816AVOC: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 88% Analysis Date = 05/27/16 SpikeMix = Phenova B20160319: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 89% Analysis Date = 04/26/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 81% Analysis Date = 03/04/16 SpikeMix = Accu 215041380: 15 µl & ERA 0406-15-03: 15 µl Pct Recovery = 77% Analysis Date = 02/05/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 91% Analysis Date = 11/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 97% Analysis Date = 10/17/15 SpikeMix = Crescent 04EE008: 15 µl & NSI 050515AVOC: 15 µl Pct Recovery = 88% Analysis Date = 10/16/15 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 83% Analysis Date = 06/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Accu 215041380: 15 µl Pct Recovery = 83% Analysis Date = 01/13/15 SpikeMix = Accu 214031115: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 81% Analysis Date = 10/21/14 SpikeMix = ERA 0227-14-06.1A: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 83% Analysis Date = 10/04/14 SpikeMix = Crescent 03DD004: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 87% Analysis Date = 07/11/14 SpikeMix = Spex Organics C1140417015: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 87% Analysis Date = 09/09/14 SpikeMix = Accu 214031115: 10 µl & NSI 032614: 10 µl Pct Recovery = 90% Analysis Date = 09/09/14 SpikeMix = NSI 032614: 10 µl & Spex Organics C1140417015: 10 µl Pct Recovery = 93% Analysis Date = 07/29/14 SpikeMix = Crescent 03DD004: 10 µl & NSI 032614: 10 µl Pct Recovery = 83% Analysis Date = 05/30/14 SpikeMix = NSI 032614: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 67% Analysis Date = 03/17/16 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 77% Analysis Date = 01/27/16 SpikeMix = Crescent 04EE008: 10 µl & NSI 050515AVOC: 10 µl Pct Recovery = 92% Analysis Date = 12/10/15 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 98% Analysis Date = 11/20/15 SpikeMix = Accu 215041380: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 83% Analysis Date = 09/03/15 SpikeMix = NSI 050515AVOC: 10 µl & Spex Organics EN150428007: 10 µl Pct Recovery = 79% Analysis Date = 07/31/15 SpikeMix = Crescent 04EE008: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 77% Analysis Date = 06/27/15 SpikeMix = ERA 0406-15-03: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 84% Analysis Date = 12/15/16 Pct Recovery = 81% Analysis Date = 12/11/16 Pct Recovery = 82% Analysis Date = 12/11/16 Pct Recovery = 82% Analysis Date = 12/06/16 Pct Recovery = 82% Analysis Date = 12/06/16 Pct Recovery = 82% Analysis Date = 12/01/16 Pct Recovery = 82% Analysis Date = 12/01/16 Pct Recovery = 82% Analysis Date = 11/26/16 Pct Recovery = 82% Analysis Date = 11/26/16 Pct Recovery = 82% Analysis Date = 11/21/16 Pct Recovery = 82% Analysis Date = 11/21/16 Pct Recovery = 82% Analysis Date = 11/17/16 Pct Recovery = 82% Analysis Date = 11/17/16 Pct Recovery = 82% Analysis Date = 11/12/16 Pct Recovery = 82% Analysis Date = 11/12/16 Pct Recovery = 82% Analysis Date = 11/07/16 Pct Recovery = 82% Analysis Date = 11/07/16 Pct Recovery = 82% Analysis Date = 11/02/16 Pct Recovery = 82% Analysis Date = 11/02/16 Pct Recovery = 82% Analysis Date = 10/28/16 Pct Recovery = 82% Analysis Date = 10/28/16 Pct Recovery = 82% Analysis Date = 10/24/16 Pct Recovery = 82% Analysis Date = 10/24/16 Pct Recovery = 82% Analysis Date = 10/19/16 Pct Recovery = 82% Analysis Date = 10/19/16 Pct Recovery = 82% Analysis Date = 10/14/16 Pct Recovery = 82% Analysis Date = 10/14/16 Pct Recovery = 82% Analysis Date = 10/09/16 Pct Recovery = 82% Analysis Date = 10/09/16 Pct Recovery = 82% Analysis Date = 10/04/16 Pct Recovery = 82% Analysis Date = 10/04/16 Pct Recovery = 82% Analysis Date = 09/30/16 Pct Recovery = 82% Analysis Date = 09/30/16 Pct Recovery = 82% Analysis Date = 09/25/16 Pct Recovery = 82% Analysis Date = 09/25/16 Pct Recovery = 82% Analysis Date = 09/20/16 Pct Recovery = 82% Analysis Date = 09/20/16 Pct Recovery = 82% Analysis Date = 09/15/16 Pct Recovery = 82% Analysis Date = 09/15/16 Pct Recovery = 82% Analysis Date = 09/10/16 Pct Recovery = 82% Analysis Date = 09/10/16 Pct Recovery = 82% Analysis Date = 09/06/16 Pct Recovery = 83% Analysis Date = 09/06/16 Pct Recovery = 83% Analysis Date = 09/01/16 Pct Recovery = 83% Analysis Date = 09/01/16 Pct Recovery = 83% Analysis Date = 08/27/16 Pct Recovery = 83% Analysis Date = 08/27/16 Pct Recovery = 83% Analysis Date = 08/22/16 Pct Recovery = 83% Analysis Date = 08/22/16 Pct Recovery = 83% Analysis Date = 08/17/16 Pct Recovery = 83% Analysis Date = 08/17/16 Pct Recovery = 83% Analysis Date = 08/13/16 Pct Recovery = 83% Analysis Date = 08/13/16 Pct Recovery = 83% Analysis Date = 08/08/16 Pct Recovery = 83% Analysis Date = 08/08/16 Pct Recovery = 83% Analysis Date = 08/03/16 Pct Recovery = 83% Analysis Date = 08/03/16 Pct Recovery = 83% Analysis Date = 07/29/16 Pct Recovery = 83% Analysis Date = 07/29/16 Pct Recovery = 83% Analysis Date = 07/24/16 Pct Recovery = 83% Analysis Date = 07/24/16 Pct Recovery = 83% Analysis Date = 07/20/16 Pct Recovery = 83% Analysis Date = 07/20/16 Pct Recovery = 83% Analysis Date = 07/15/16 Pct Recovery = 83% Analysis Date = 07/15/16 Pct Recovery = 83% Analysis Date = 07/10/16 Pct Recovery = 83% Analysis Date = 07/10/16 Pct Recovery = 83% Analysis Date = 07/05/16 Pct Recovery = 83% Analysis Date = 07/05/16 Pct Recovery = 83% Analysis Date = 06/30/16 Pct Recovery = 83% Analysis Date = 06/30/16 Pct Recovery = 83% Analysis Date = 06/26/16 Pct Recovery = 83% Analysis Date = 06/26/16 Pct Recovery = 83% Analysis Date = 06/21/16 Pct Recovery = 83% Analysis Date = 06/21/16 Pct Recovery = 83% Analysis Date = 06/16/16 Pct Recovery = 84% Analysis Date = 06/16/16 Pct Recovery = 84% Analysis Date = 06/11/16 Pct Recovery = 84% Analysis Date = 06/11/16 Pct Recovery = 84% Analysis Date = 06/06/16 Pct Recovery = 84% Analysis Date = 06/06/16 Pct Recovery = 84% Analysis Date = 06/02/16 Pct Recovery = 84% Analysis Date = 06/02/16 Pct Recovery = 84% Analysis Date = 05/28/16 Pct Recovery = 84% Analysis Date = 05/28/16 Pct Recovery = 84% Analysis Date = 05/23/16 Pct Recovery = 84% Analysis Date = 05/23/16 Pct Recovery = 84% Analysis Date = 05/18/16 Pct Recovery = 84% Analysis Date = 05/18/16 Pct Recovery = 84% Analysis Date = 05/13/16 Pct Recovery = 84% Analysis Date = 05/13/16 Pct Recovery = 84% Analysis Date = 05/09/16 Pct Recovery = 84% Analysis Date = 05/09/16 Pct Recovery = 84% Analysis Date = 05/04/16 Pct Recovery = 84% Analysis Date = 05/04/16 Pct Recovery = 84% Analysis Date = 04/29/16 Pct Recovery = 84% Analysis Date = 04/29/16 Pct Recovery = 84% Analysis Date = 04/24/16 Pct Recovery = 84% Analysis Date = 04/24/16 Pct Recovery = 84% Analysis Date = 04/19/16 Pct Recovery = 85% Analysis Date = 04/19/16 Pct Recovery = 85% Analysis Date = 04/15/16 Pct Recovery = 85% Analysis Date = 04/15/16 Pct Recovery = 85% Analysis Date = 04/10/16 Pct Recovery = 85% Analysis Date = 04/10/16 Pct Recovery = 85% Analysis Date = 04/05/16 Pct Recovery = 85% Analysis Date = 04/05/16 Pct Recovery = 85% Analysis Date = 03/31/16 Pct Recovery = 85% Analysis Date = 03/31/16 Pct Recovery = 85% Analysis Date = 03/26/16 Pct Recovery = 85% Analysis Date = 03/26/16 Pct Recovery = 85% Analysis Date = 03/22/16 Pct Recovery = 85% Analysis Date = 03/22/16 Pct Recovery = 85% Analysis Date = 03/17/16 Pct Recovery = 85% Analysis Date = 03/17/16 Pct Recovery = 85% Analysis Date = 03/12/16 Pct Recovery = 85% Analysis Date = 03/12/16 Pct Recovery = 85% Analysis Date = 03/07/16 Pct Recovery = 85% Analysis Date = 03/07/16 Pct Recovery = 85% Analysis Date = 03/02/16 Pct Recovery = 85% Analysis Date = 03/02/16 Pct Recovery = 85% Analysis Date = 02/27/16 Pct Recovery = 85% Analysis Date = 02/27/16 Pct Recovery = 85% Analysis Date = 02/22/16 Pct Recovery = 85% Analysis Date = 02/22/16 Pct Recovery = 85% Analysis Date = 02/17/16 Pct Recovery = 85% Analysis Date = 02/17/16 Pct Recovery = 85% Analysis Date = 02/12/16 Pct Recovery = 85% Analysis Date = 02/12/16 Pct Recovery = 85% Analysis Date = 02/07/16 Pct Recovery = 85% Analysis Date = 02/07/16 Pct Recovery = 85% Analysis Date = 02/03/16 Pct Recovery = 85% Analysis Date = 02/03/16 Pct Recovery = 85% Analysis Date = 01/29/16 Pct Recovery = 85% Analysis Date = 01/29/16 Pct Recovery = 85% Analysis Date = 01/24/16 Pct Recovery = 85% Analysis Date = 01/24/16 Pct Recovery = 85% Analysis Date = 01/19/16 Pct Recovery = 85% Analysis Date = 01/19/16 Pct Recovery = 85% Analysis Date = 01/14/16 Pct Recovery = 85% Analysis Date = 01/14/16 Pct Recovery = 85% Analysis Date = 01/10/16 Pct Recovery = 85% Analysis Date = 01/10/16 Pct Recovery = 85% Analysis Date = 01/05/16 Pct Recovery = 85% Analysis Date = 01/05/16 Pct Recovery = 85% Analysis Date = 12/31/15 Pct Recovery = 85% Analysis Date = 12/31/15 Pct Recovery = 85% Analysis Date = 12/26/15 Pct Recovery = 85% Analysis Date = 12/26/15 Pct Recovery = 85% Analysis Date = 12/21/15 Pct Recovery = 85% Analysis Date = 12/21/15 Pct Recovery = 85% Analysis Date = 12/17/15 Pct Recovery = 85% Analysis Date = 12/17/15 Pct Recovery = 85% Analysis Date = 12/12/15 Pct Recovery = 85% Analysis Date = 12/12/15 Pct Recovery = 85% Analysis Date = 12/07/15 Pct Recovery = 85% Analysis Date = 12/07/15 Pct Recovery = 85% Analysis Date = 12/02/15 Pct Recovery = 85% Analysis Date = 12/02/15 Pct Recovery = 85% Analysis Date = 11/27/15 Pct Recovery = 85% Analysis Date = 11/27/15 Pct Recovery = 85% Analysis Date = 11/23/15 Pct Recovery = 85% Analysis Date = 11/23/15 Pct Recovery = 85% Analysis Date = 11/18/15 Pct Recovery = 85% Analysis Date = 11/18/15 Pct Recovery = 85% Analysis Date = 11/13/15 Pct Recovery = 85% Analysis Date = 11/13/15 Pct Recovery = 85% Analysis Date = 11/08/15 Pct Recovery = 85% Analysis Date = 11/08/15 Pct Recovery = 85% Analysis Date = 11/03/15 Pct Recovery = 85% Analysis Date = 11/03/15 Pct Recovery = 85% Analysis Date = 10/30/15 Pct Recovery = 85% Analysis Date = 10/30/15 Pct Recovery = 85% Analysis Date = 10/25/15 Pct Recovery = 85% Analysis Date = 10/25/15 Pct Recovery = 85% Analysis Date = 10/20/15 Pct Recovery = 85% Analysis Date = 10/20/15 Pct Recovery = 85% Analysis Date = 10/15/15 Pct Recovery = 85% Analysis Date = 10/15/15 Pct Recovery = 85% Analysis Date = 10/10/15 Pct Recovery = 85% Analysis Date = 10/10/15 Pct Recovery = 85% Analysis Date = 10/06/15 Pct Recovery = 85% Analysis Date = 10/06/15 Pct Recovery = 85% Analysis Date = 10/01/15 Pct Recovery = 84% Analysis Date = 10/01/15 Pct Recovery = 84% Analysis Date = 09/26/15 Pct Recovery = 84% Analysis Date = 09/26/15 Pct Recovery = 84% Analysis Date = 09/21/15 Pct Recovery = 84% Analysis Date = 09/21/15 Pct Recovery = 84% Analysis Date = 09/16/15 Pct Recovery = 84% Analysis Date = 09/16/15 Pct Recovery = 84% Analysis Date = 09/12/15 Pct Recovery = 84% Analysis Date = 09/12/15 Pct Recovery = 84% Analysis Date = 09/07/15 Pct Recovery = 84% Analysis Date = 09/07/15 Pct Recovery = 84% Analysis Date = 09/02/15 Pct Recovery = 84% Analysis Date = 09/02/15 Pct Recovery = 84% Analysis Date = 08/28/15 Pct Recovery = 84% Analysis Date = 08/28/15 Pct Recovery = 84% Analysis Date = 08/23/15 Pct Recovery = 84% Analysis Date = 08/23/15 Pct Recovery = 84% Analysis Date = 08/19/15 Pct Recovery = 84% Analysis Date = 08/19/15 Pct Recovery = 84% Analysis Date = 08/14/15 Pct Recovery = 84% Analysis Date = 08/14/15 Pct Recovery = 84% Analysis Date = 08/09/15 Pct Recovery = 84% Analysis Date = 08/09/15 Pct Recovery = 84% Analysis Date = 08/04/15 Pct Recovery = 84% Analysis Date = 08/04/15 Pct Recovery = 84% Analysis Date = 07/30/15 Pct Recovery = 84% Analysis Date = 07/30/15 Pct Recovery = 84% Analysis Date = 07/26/15 Pct Recovery = 84% Analysis Date = 07/26/15 Pct Recovery = 84% Analysis Date = 07/21/15 Pct Recovery = 84% Analysis Date = 07/21/15 Pct Recovery = 84% Analysis Date = 07/16/15 Pct Recovery = 84% Analysis Date = 07/16/15 Pct Recovery = 84% Analysis Date = 07/11/15 Pct Recovery = 84% Analysis Date = 07/11/15 Pct Recovery = 84% Analysis Date = 07/06/15 Pct Recovery = 84% Analysis Date = 07/06/15 Pct Recovery = 84% Analysis Date = 07/02/15 Pct Recovery = 84% Analysis Date = 07/02/15 Pct Recovery = 84% Analysis Date = 06/27/15 Pct Recovery = 84% Analysis Date = 06/27/15 Pct Recovery = 84% Analysis Date = 06/22/15 Pct Recovery = 84% Analysis Date = 06/22/15 Pct Recovery = 84% Analysis Date = 06/17/15 Pct Recovery = 84% Analysis Date = 06/17/15 Pct Recovery = 84% Analysis Date = 06/12/15 Pct Recovery = 84% Analysis Date = 06/12/15 Pct Recovery = 84% Analysis Date = 06/08/15 Pct Recovery = 83% Analysis Date = 06/08/15 Pct Recovery = 83% Analysis Date = 06/03/15 Pct Recovery = 83% Analysis Date = 06/03/15 Pct Recovery = 83% Analysis Date = 05/29/15 Pct Recovery = 83% Analysis Date = 05/29/15 Pct Recovery = 83% Analysis Date = 05/24/15 Pct Recovery = 83% Analysis Date = 05/24/15 Pct Recovery = 83% Analysis Date = 05/19/15 Pct Recovery = 83% Analysis Date = 05/19/15 Pct Recovery = 83% Analysis Date = 05/15/15 Pct Recovery = 83% Analysis Date = 05/15/15 Pct Recovery = 83% Analysis Date = 05/10/15 Pct Recovery = 83% Analysis Date = 05/10/15 Pct Recovery = 83% Analysis Date = 05/05/15 Pct Recovery = 83% Analysis Date = 05/05/15 Pct Recovery = 83% Analysis Date = 04/30/15 Pct Recovery = 83% Analysis Date = 04/30/15 Pct Recovery = 83% Analysis Date = 04/25/15 Pct Recovery = 83% Analysis Date = 04/25/15 Pct Recovery = 83% Analysis Date = 04/21/15 Pct Recovery = 83% Analysis Date = 04/21/15 Pct Recovery = 83% Analysis Date = 04/16/15 Pct Recovery = 83% Analysis Date = 04/16/15 Pct Recovery = 83% Analysis Date = 04/11/15 Pct Recovery = 83% Analysis Date = 04/11/15 Pct Recovery = 83% Analysis Date = 04/06/15 Pct Recovery = 83% Analysis Date = 04/06/15 Pct Recovery = 83% Analysis Date = 04/01/15 Pct Recovery = 83% Analysis Date = 04/01/15 Pct Recovery = 83% Analysis Date = 03/28/15 Pct Recovery = 83% Analysis Date = 03/28/15 Pct Recovery = 83% Analysis Date = 03/23/15 Pct Recovery = 83% Analysis Date = 03/23/15 Pct Recovery = 83% Analysis Date = 03/18/15 Pct Recovery = 83% Analysis Date = 03/18/15 Pct Recovery = 83% Analysis Date = 03/13/15 Pct Recovery = 83% Analysis Date = 03/13/15 Pct Recovery = 83% Analysis Date = 03/08/15 Pct Recovery = 83% Analysis Date = 03/08/15 Pct Recovery = 83% Analysis Date = 03/04/15 Pct Recovery = 83% Analysis Date = 03/04/15 Pct Recovery = 83% Analysis Date = 02/27/15 Pct Recovery = 83% Analysis Date = 02/27/15 Pct Recovery = 83% Analysis Date = 02/22/15 Pct Recovery = 83% Analysis Date = 02/22/15 Pct Recovery = 83% Analysis Date = 02/17/15 Pct Recovery = 83% Analysis Date = 02/17/15 Pct Recovery = 83% Analysis Date = 02/12/15 Pct Recovery = 83% Analysis Date = 02/12/15 Pct Recovery = 83% Analysis Date = 02/08/15 Pct Recovery = 83% Analysis Date = 02/08/15 Pct Recovery = 83% Analysis Date = 02/03/15 Pct Recovery = 83% Analysis Date = 02/03/15 Pct Recovery = 83% Analysis Date = 01/29/15 Pct Recovery = 83% Analysis Date = 01/29/15 Pct Recovery = 83% Analysis Date = 01/24/15 Pct Recovery = 83% Analysis Date = 01/24/15 Pct Recovery = 83% Analysis Date = 01/19/15 Pct Recovery = 83% Analysis Date = 01/19/15 Pct Recovery = 83% Analysis Date = 01/15/15 Pct Recovery = 83% Analysis Date = 01/15/15 Pct Recovery = 83% Analysis Date = 01/10/15 Pct Recovery = 83% Analysis Date = 01/10/15 Pct Recovery = 83% Analysis Date = 01/05/15 Pct Recovery = 83% Analysis Date = 01/05/15 Pct Recovery = 83% Analysis Date = 12/31/14 Pct Recovery = 82% Analysis Date = 12/31/14 Pct Recovery = 82% Analysis Date = 12/26/14 Pct Recovery = 82% Analysis Date = 12/26/14 Pct Recovery = 82% Analysis Date = 12/22/14 Pct Recovery = 82% Analysis Date = 12/22/14 Pct Recovery = 82% Analysis Date = 12/17/14 Pct Recovery = 82% Analysis Date = 12/17/14 Pct Recovery = 82% Analysis Date = 12/12/14 Pct Recovery = 82% Analysis Date = 12/12/14 Pct Recovery = 82% Analysis Date = 12/07/14 Pct Recovery = 82% Analysis Date = 12/07/14 Pct Recovery = 82% Analysis Date = 12/02/14 Pct Recovery = 82% Analysis Date = 12/02/14 Pct Recovery = 82% Analysis Date = 11/28/14 Pct Recovery = 82% Analysis Date = 11/28/14 Pct Recovery = 82% Analysis Date = 11/23/14 Pct Recovery = 82% Analysis Date = 11/23/14 Pct Recovery = 82% Analysis Date = 11/18/14 Pct Recovery = 82% Analysis Date = 11/18/14 Pct Recovery = 82% Analysis Date = 11/13/14 Pct Recovery = 82% Analysis Date = 11/13/14 Pct Recovery = 82% Analysis Date = 11/08/14 Pct Recovery = 82% Analysis Date = 11/08/14 Pct Recovery = 82% Analysis Date = 11/04/14 Pct Recovery = 82% Analysis Date = 11/04/14 Pct Recovery = 82% Analysis Date = 10/30/14 Pct Recovery = 81% Analysis Date = 10/30/14 Pct Recovery = 81% Analysis Date = 10/25/14 Pct Recovery = 81% Analysis Date = 10/25/14 Pct Recovery = 81% Analysis Date = 10/20/14 Pct Recovery = 81% Analysis Date = 10/20/14 Pct Recovery = 81% Analysis Date = 10/15/14 Pct Recovery = 81% Analysis Date = 10/15/14 Pct Recovery = 81% Analysis Date = 10/11/14 Pct Recovery = 81% Analysis Date = 10/11/14 Pct Recovery = 81% Analysis Date = 10/06/14 Pct Recovery = 81% Analysis Date = 10/06/14 Pct Recovery = 81% Analysis Date = 10/01/14 Pct Recovery = 81% Analysis Date = 10/01/14 Pct Recovery = 81% Analysis Date = 09/26/14 Pct Recovery = 81% Analysis Date = 09/26/14 Pct Recovery = 81% Analysis Date = 09/21/14 Pct Recovery = 81% Analysis Date = 09/21/14 Pct Recovery = 81% Analysis Date = 09/17/14 Pct Recovery = 81% Analysis Date = 09/17/14 Pct Recovery = 81% Analysis Date = 09/12/14 Pct Recovery = 81% Analysis Date = 09/12/14 Pct Recovery = 81% Analysis Date = 09/07/14 Pct Recovery = 80% Analysis Date = 09/07/14 Pct Recovery = 80% Analysis Date = 09/02/14 Pct Recovery = 80% Analysis Date = 09/02/14 Pct Recovery = 80% Analysis Date = 08/28/14 Pct Recovery = 80% Analysis Date = 08/28/14 Pct Recovery = 80% Analysis Date = 08/24/14 Pct Recovery = 80% Analysis Date = 08/24/14 Pct Recovery = 80% Analysis Date = 08/19/14 Pct Recovery = 80% Analysis Date = 08/19/14 Pct Recovery = 80% Analysis Date = 08/14/14 Pct Recovery = 80% Analysis Date = 08/14/14 Pct Recovery = 80% Analysis Date = 08/09/14 Pct Recovery = 80% Analysis Date = 08/09/14 Pct Recovery = 80% Analysis Date = 08/04/14 Pct Recovery = 80% Analysis Date = 08/04/14 Pct Recovery = 80% Analysis Date = 07/31/14 Pct Recovery = 80% Analysis Date = 07/31/14 Pct Recovery = 80% Analysis Date = 07/26/14 Pct Recovery = 80% Analysis Date = 07/26/14 Pct Recovery = 80% Analysis Date = 07/21/14 Pct Recovery = 79% Analysis Date = 07/21/14 Pct Recovery = 79% Analysis Date = 07/16/14 Pct Recovery = 79% Analysis Date = 07/16/14 Pct Recovery = 79% Analysis Date = 07/11/14 Pct Recovery = 79% Analysis Date = 07/11/14 Pct Recovery = 79% Analysis Date = 07/07/14 Pct Recovery = 79% Analysis Date = 07/07/14 Pct Recovery = 79% Analysis Date = 07/02/14 Pct Recovery = 79% Analysis Date = 07/02/14 Pct Recovery = 79% Analysis Date = 06/27/14 Pct Recovery = 79% Analysis Date = 06/27/14 Pct Recovery = 79% Analysis Date = 06/22/14 Pct Recovery = 79% Analysis Date = 06/22/14 Pct Recovery = 79% Analysis Date = 06/17/14 Pct Recovery = 79% Analysis Date = 06/17/14 Pct Recovery = 79% Analysis Date = 06/13/14 Pct Recovery = 79% Analysis Date = 06/13/14 Pct Recovery = 79% Analysis Date = 06/08/14 Pct Recovery = 78% Analysis Date = 06/08/14 Pct Recovery = 78% Analysis Date = 06/03/14 Pct Recovery = 78% Analysis Date = 06/03/14 Pct Recovery = 78% Analysis Date = 05/29/14 Pct Recovery = 78% Analysis Date = 05/29/14 Pct Recovery = 78% Analysis Date = 05/24/14 Pct Recovery = 78% Analysis Date = 05/24/14 Pct Recovery = 78% Analysis Date = 05/20/14 Pct Recovery = 78% Analysis Date = 05/20/14 Pct Recovery = 78% Analysis Date = 05/15/14 Pct Recovery = 78% Analysis Date = 05/15/14 Pct Recovery = 78% Analysis Date = 05/10/14 Pct Recovery = 78% Analysis Date = 05/10/14 Pct Recovery = 78% Analysis Date = 05/05/14 Pct Recovery = 78% Analysis Date = 05/05/14 Pct Recovery = 78% Analysis Date = 05/01/14 Pct Recovery = 77% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
1,2,3-TRIMETHYLBENZENE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 48 83% 8% 83% 8%
Total 48 83% 8% 83% 8%

Sample Statistics
1,2,3-TRIMETHYLBENZENE

Characteristic N % % Basis
Plotted 48 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 48 .  
False Negatives 0 0% 0 out of 48
Not Spiked 25 .  
False Positives 0 0% 0 out of 25

BQS OBSP Determination:
1,2,4-TRICHLOROBENZENE
METHOD: 4440 , TESTIDCODE: 34551GCM66
Open Data Set

Analysis Date = 12/12/16 SpikeMix = Accu 216041125: 40 µl & Crescent 03FF058: 40 µl Pct Recovery = 92% Analysis Date = 07/20/16 SpikeMix = Supelco LC20141V: 40 µl & Accu 216041125: 40 µl Pct Recovery = 89% Analysis Date = 07/14/16 SpikeMix = Accu 216041125: 40 µl & NSI 041816AVOC: 40 µl Pct Recovery = 78% Analysis Date = 08/12/16 SpikeMix = ChemService 5082900: 25 µl & Phenova B20160319: 25 µl Pct Recovery = 86% Analysis Date = 06/21/16 SpikeMix = Phenova B20160319: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 92% Analysis Date = 09/08/16 SpikeMix = Supelco LC20141V: 25 µl & Accu 216041125: 25 µl Pct Recovery = 74% Analysis Date = 05/24/16 SpikeMix = Accu 216041125: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 84% Analysis Date = 03/06/15 SpikeMix = ERA 0227-14-06.1A: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 79% Analysis Date = 12/17/14 SpikeMix = Supelco LC06438: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 78% Analysis Date = 09/21/14 SpikeMix = Supelco LC06438: 20 µl Pct Recovery = 66% Analysis Date = 06/10/14 SpikeMix = NSI 032614: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 87% Analysis Date = 03/19/15 SpikeMix = Spex Organics C1140417015: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 100% Analysis Date = 11/22/14 SpikeMix = NSI 032614: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 93% Analysis Date = 08/19/14 SpikeMix = Spex Organics C1140417015: 20 µl & Accu 214031115: 20 µl Pct Recovery = 95% Analysis Date = 08/16/14 SpikeMix = ERA 0227-14-06.1A: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 86% Analysis Date = 08/15/15 SpikeMix = Supelco LC13545: 25 µl & Crescent 04EE008: 25 µl Pct Recovery = 96% Analysis Date = 06/16/15 SpikeMix = ERA 0406-15-03: 25 µl & Supelco LC13545: 25 µl Pct Recovery = 94% Analysis Date = 11/29/16 SpikeMix = ChemService 5082900: 15 µl & Phenova B20160319: 15 µl Pct Recovery = 81% Analysis Date = 09/08/16 SpikeMix = Phenova B20160319: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 88% Analysis Date = 07/29/16 SpikeMix = Phenova B20160319: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 80% Analysis Date = 05/27/16 SpikeMix = Phenova B20160319: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 97% Analysis Date = 10/13/16 SpikeMix = Accu 216041125: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 81% Analysis Date = 08/20/16 SpikeMix = Accu 216041125: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 87% Analysis Date = 06/30/16 SpikeMix = ChemService 5082900: 15 µl & Accu 216041125: 15 µl Pct Recovery = 64% Analysis Date = 04/26/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 96% Analysis Date = 04/02/16 SpikeMix = Supelco LC13545: 15 µl & Accu 215041380: 15 µl Pct Recovery = 84% Analysis Date = 02/05/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 82% Analysis Date = 12/18/15 SpikeMix = Supelco LC13545: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 99% Analysis Date = 11/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 94% Analysis Date = 10/16/15 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 94% Analysis Date = 05/09/15 SpikeMix = Spex Organics EN150428007: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 89% Analysis Date = 10/21/14 SpikeMix = ERA 0227-14-06.1A: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 84% Analysis Date = 06/18/14 SpikeMix = Supelco LC06438: 10 µl & Accu 214031115: 10 µl Pct Recovery = 84% Analysis Date = 05/30/14 SpikeMix = NSI 032614: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 60% Analysis Date = 05/03/14 SpikeMix = Crescent 03DD004: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 80% Analysis Date = 11/06/14 SpikeMix = Spex Organics C1140417015: 10 µl & Crescent 03DD004: 10 µl Pct Recovery = 97% Analysis Date = 09/09/14 SpikeMix = NSI 032614: 10 µl & Spex Organics C1140417015: 10 µl Pct Recovery = 108% Analysis Date = 07/23/14 SpikeMix = Spex Organics C1140417015: 10 µl & Accu 214031115: 10 µl Pct Recovery = 99% Analysis Date = 07/11/14 SpikeMix = Spex Organics C1140417015: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 90% Analysis Date = 05/13/16 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 93% Analysis Date = 03/17/16 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 83% Analysis Date = 02/18/16 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 88% Analysis Date = 12/10/15 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 87% Analysis Date = 11/12/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 89% Analysis Date = 09/03/15 SpikeMix = NSI 050515AVOC: 10 µl & Spex Organics EN150428007: 10 µl Pct Recovery = 85% Analysis Date = 06/27/15 SpikeMix = ERA 0406-15-03: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 96% Analysis Date = 05/21/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 95% Analysis Date = 05/09/15 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 88% Analysis Date = 12/12/16 Pct Recovery = 82% Analysis Date = 12/07/16 Pct Recovery = 82% Analysis Date = 12/07/16 Pct Recovery = 82% Analysis Date = 12/02/16 Pct Recovery = 82% Analysis Date = 12/02/16 Pct Recovery = 82% Analysis Date = 11/27/16 Pct Recovery = 82% Analysis Date = 11/27/16 Pct Recovery = 82% Analysis Date = 11/22/16 Pct Recovery = 82% Analysis Date = 11/22/16 Pct Recovery = 82% Analysis Date = 11/18/16 Pct Recovery = 82% Analysis Date = 11/18/16 Pct Recovery = 82% Analysis Date = 11/13/16 Pct Recovery = 83% Analysis Date = 11/13/16 Pct Recovery = 83% Analysis Date = 11/08/16 Pct Recovery = 83% Analysis Date = 11/08/16 Pct Recovery = 83% Analysis Date = 11/03/16 Pct Recovery = 83% Analysis Date = 11/03/16 Pct Recovery = 83% Analysis Date = 10/30/16 Pct Recovery = 83% Analysis Date = 10/30/16 Pct Recovery = 83% Analysis Date = 10/25/16 Pct Recovery = 83% Analysis Date = 10/25/16 Pct Recovery = 83% Analysis Date = 10/20/16 Pct Recovery = 83% Analysis Date = 10/20/16 Pct Recovery = 83% Analysis Date = 10/15/16 Pct Recovery = 83% Analysis Date = 10/15/16 Pct Recovery = 83% Analysis Date = 10/10/16 Pct Recovery = 83% Analysis Date = 10/10/16 Pct Recovery = 83% Analysis Date = 10/06/16 Pct Recovery = 83% Analysis Date = 10/06/16 Pct Recovery = 83% Analysis Date = 10/01/16 Pct Recovery = 83% Analysis Date = 10/01/16 Pct Recovery = 83% Analysis Date = 09/26/16 Pct Recovery = 83% Analysis Date = 09/26/16 Pct Recovery = 83% Analysis Date = 09/21/16 Pct Recovery = 84% Analysis Date = 09/21/16 Pct Recovery = 84% Analysis Date = 09/17/16 Pct Recovery = 84% Analysis Date = 09/17/16 Pct Recovery = 84% Analysis Date = 09/12/16 Pct Recovery = 84% Analysis Date = 09/12/16 Pct Recovery = 84% Analysis Date = 09/07/16 Pct Recovery = 84% Analysis Date = 09/07/16 Pct Recovery = 84% Analysis Date = 09/02/16 Pct Recovery = 84% Analysis Date = 09/02/16 Pct Recovery = 84% Analysis Date = 08/29/16 Pct Recovery = 84% Analysis Date = 08/29/16 Pct Recovery = 84% Analysis Date = 08/24/16 Pct Recovery = 84% Analysis Date = 08/24/16 Pct Recovery = 84% Analysis Date = 08/19/16 Pct Recovery = 84% Analysis Date = 08/19/16 Pct Recovery = 84% Analysis Date = 08/14/16 Pct Recovery = 84% Analysis Date = 08/14/16 Pct Recovery = 84% Analysis Date = 08/09/16 Pct Recovery = 84% Analysis Date = 08/09/16 Pct Recovery = 84% Analysis Date = 08/05/16 Pct Recovery = 84% Analysis Date = 08/05/16 Pct Recovery = 84% Analysis Date = 07/31/16 Pct Recovery = 85% Analysis Date = 07/31/16 Pct Recovery = 85% Analysis Date = 07/26/16 Pct Recovery = 85% Analysis Date = 07/26/16 Pct Recovery = 85% Analysis Date = 07/21/16 Pct Recovery = 85% Analysis Date = 07/21/16 Pct Recovery = 85% Analysis Date = 07/17/16 Pct Recovery = 85% Analysis Date = 07/17/16 Pct Recovery = 85% Analysis Date = 07/12/16 Pct Recovery = 85% Analysis Date = 07/12/16 Pct Recovery = 85% Analysis Date = 07/07/16 Pct Recovery = 85% Analysis Date = 07/07/16 Pct Recovery = 85% Analysis Date = 07/02/16 Pct Recovery = 85% Analysis Date = 07/02/16 Pct Recovery = 85% Analysis Date = 06/28/16 Pct Recovery = 85% Analysis Date = 06/28/16 Pct Recovery = 85% Analysis Date = 06/23/16 Pct Recovery = 85% Analysis Date = 06/23/16 Pct Recovery = 85% Analysis Date = 06/18/16 Pct Recovery = 85% Analysis Date = 06/18/16 Pct Recovery = 85% Analysis Date = 06/13/16 Pct Recovery = 86% Analysis Date = 06/13/16 Pct Recovery = 86% Analysis Date = 06/08/16 Pct Recovery = 86% Analysis Date = 06/08/16 Pct Recovery = 86% Analysis Date = 06/04/16 Pct Recovery = 86% Analysis Date = 06/04/16 Pct Recovery = 86% Analysis Date = 05/30/16 Pct Recovery = 86% Analysis Date = 05/30/16 Pct Recovery = 86% Analysis Date = 05/25/16 Pct Recovery = 86% Analysis Date = 05/25/16 Pct Recovery = 86% Analysis Date = 05/20/16 Pct Recovery = 86% Analysis Date = 05/20/16 Pct Recovery = 86% Analysis Date = 05/16/16 Pct Recovery = 86% Analysis Date = 05/16/16 Pct Recovery = 86% Analysis Date = 05/11/16 Pct Recovery = 86% Analysis Date = 05/11/16 Pct Recovery = 86% Analysis Date = 05/06/16 Pct Recovery = 86% Analysis Date = 05/06/16 Pct Recovery = 86% Analysis Date = 05/01/16 Pct Recovery = 87% Analysis Date = 05/01/16 Pct Recovery = 87% Analysis Date = 04/27/16 Pct Recovery = 87% Analysis Date = 04/27/16 Pct Recovery = 87% Analysis Date = 04/22/16 Pct Recovery = 87% Analysis Date = 04/22/16 Pct Recovery = 87% Analysis Date = 04/17/16 Pct Recovery = 87% Analysis Date = 04/17/16 Pct Recovery = 87% Analysis Date = 04/12/16 Pct Recovery = 87% Analysis Date = 04/12/16 Pct Recovery = 87% Analysis Date = 04/07/16 Pct Recovery = 87% Analysis Date = 04/07/16 Pct Recovery = 87% Analysis Date = 04/03/16 Pct Recovery = 87% Analysis Date = 04/03/16 Pct Recovery = 87% Analysis Date = 03/29/16 Pct Recovery = 87% Analysis Date = 03/29/16 Pct Recovery = 87% Analysis Date = 03/24/16 Pct Recovery = 88% Analysis Date = 03/24/16 Pct Recovery = 88% Analysis Date = 03/19/16 Pct Recovery = 88% Analysis Date = 03/19/16 Pct Recovery = 88% Analysis Date = 03/15/16 Pct Recovery = 88% Analysis Date = 03/15/16 Pct Recovery = 88% Analysis Date = 03/10/16 Pct Recovery = 88% Analysis Date = 03/10/16 Pct Recovery = 88% Analysis Date = 03/05/16 Pct Recovery = 88% Analysis Date = 03/05/16 Pct Recovery = 88% Analysis Date = 02/29/16 Pct Recovery = 88% Analysis Date = 02/29/16 Pct Recovery = 88% Analysis Date = 02/25/16 Pct Recovery = 88% Analysis Date = 02/25/16 Pct Recovery = 88% Analysis Date = 02/20/16 Pct Recovery = 89% Analysis Date = 02/20/16 Pct Recovery = 89% Analysis Date = 02/15/16 Pct Recovery = 89% Analysis Date = 02/15/16 Pct Recovery = 89% Analysis Date = 02/10/16 Pct Recovery = 89% Analysis Date = 02/10/16 Pct Recovery = 89% Analysis Date = 02/05/16 Pct Recovery = 89% Analysis Date = 02/05/16 Pct Recovery = 89% Analysis Date = 02/01/16 Pct Recovery = 89% Analysis Date = 02/01/16 Pct Recovery = 89% Analysis Date = 01/27/16 Pct Recovery = 89% Analysis Date = 01/27/16 Pct Recovery = 89% Analysis Date = 01/22/16 Pct Recovery = 89% Analysis Date = 01/22/16 Pct Recovery = 89% Analysis Date = 01/17/16 Pct Recovery = 89% Analysis Date = 01/17/16 Pct Recovery = 89% Analysis Date = 01/13/16 Pct Recovery = 89% Analysis Date = 01/13/16 Pct Recovery = 89% Analysis Date = 01/08/16 Pct Recovery = 90% Analysis Date = 01/08/16 Pct Recovery = 90% Analysis Date = 01/03/16 Pct Recovery = 90% Analysis Date = 01/03/16 Pct Recovery = 90% Analysis Date = 12/29/15 Pct Recovery = 90% Analysis Date = 12/29/15 Pct Recovery = 90% Analysis Date = 12/25/15 Pct Recovery = 90% Analysis Date = 12/25/15 Pct Recovery = 90% Analysis Date = 12/20/15 Pct Recovery = 90% Analysis Date = 12/20/15 Pct Recovery = 90% Analysis Date = 12/15/15 Pct Recovery = 90% Analysis Date = 12/15/15 Pct Recovery = 90% Analysis Date = 12/10/15 Pct Recovery = 90% Analysis Date = 12/10/15 Pct Recovery = 90% Analysis Date = 12/05/15 Pct Recovery = 90% Analysis Date = 12/05/15 Pct Recovery = 90% Analysis Date = 12/01/15 Pct Recovery = 90% Analysis Date = 12/01/15 Pct Recovery = 90% Analysis Date = 11/26/15 Pct Recovery = 90% Analysis Date = 11/26/15 Pct Recovery = 90% Analysis Date = 11/21/15 Pct Recovery = 90% Analysis Date = 11/21/15 Pct Recovery = 90% Analysis Date = 11/16/15 Pct Recovery = 91% Analysis Date = 11/16/15 Pct Recovery = 91% Analysis Date = 11/12/15 Pct Recovery = 91% Analysis Date = 11/12/15 Pct Recovery = 91% Analysis Date = 11/07/15 Pct Recovery = 91% Analysis Date = 11/07/15 Pct Recovery = 91% Analysis Date = 11/02/15 Pct Recovery = 91% Analysis Date = 11/02/15 Pct Recovery = 91% Analysis Date = 10/28/15 Pct Recovery = 91% Analysis Date = 10/28/15 Pct Recovery = 91% Analysis Date = 10/24/15 Pct Recovery = 91% Analysis Date = 10/24/15 Pct Recovery = 91% Analysis Date = 10/19/15 Pct Recovery = 91% Analysis Date = 10/19/15 Pct Recovery = 91% Analysis Date = 10/14/15 Pct Recovery = 91% Analysis Date = 10/14/15 Pct Recovery = 91% Analysis Date = 10/09/15 Pct Recovery = 91% Analysis Date = 10/09/15 Pct Recovery = 91% Analysis Date = 10/04/15 Pct Recovery = 91% Analysis Date = 10/04/15 Pct Recovery = 91% Analysis Date = 09/30/15 Pct Recovery = 91% Analysis Date = 09/30/15 Pct Recovery = 91% Analysis Date = 09/25/15 Pct Recovery = 91% Analysis Date = 09/25/15 Pct Recovery = 91% Analysis Date = 09/20/15 Pct Recovery = 91% Analysis Date = 09/20/15 Pct Recovery = 91% Analysis Date = 09/15/15 Pct Recovery = 91% Analysis Date = 09/15/15 Pct Recovery = 91% Analysis Date = 09/11/15 Pct Recovery = 91% Analysis Date = 09/11/15 Pct Recovery = 91% Analysis Date = 09/06/15 Pct Recovery = 91% Analysis Date = 09/06/15 Pct Recovery = 91% Analysis Date = 09/01/15 Pct Recovery = 91% Analysis Date = 09/01/15 Pct Recovery = 91% Analysis Date = 08/27/15 Pct Recovery = 91% Analysis Date = 08/27/15 Pct Recovery = 91% Analysis Date = 08/23/15 Pct Recovery = 91% Analysis Date = 08/23/15 Pct Recovery = 91% Analysis Date = 08/18/15 Pct Recovery = 91% Analysis Date = 08/18/15 Pct Recovery = 91% Analysis Date = 08/13/15 Pct Recovery = 91% Analysis Date = 08/13/15 Pct Recovery = 91% Analysis Date = 08/08/15 Pct Recovery = 91% Analysis Date = 08/08/15 Pct Recovery = 91% Analysis Date = 08/03/15 Pct Recovery = 91% Analysis Date = 08/03/15 Pct Recovery = 91% Analysis Date = 07/30/15 Pct Recovery = 91% Analysis Date = 07/30/15 Pct Recovery = 91% Analysis Date = 07/25/15 Pct Recovery = 91% Analysis Date = 07/25/15 Pct Recovery = 91% Analysis Date = 07/20/15 Pct Recovery = 91% Analysis Date = 07/20/15 Pct Recovery = 91% Analysis Date = 07/15/15 Pct Recovery = 91% Analysis Date = 07/15/15 Pct Recovery = 91% Analysis Date = 07/11/15 Pct Recovery = 91% Analysis Date = 07/11/15 Pct Recovery = 91% Analysis Date = 07/06/15 Pct Recovery = 91% Analysis Date = 07/06/15 Pct Recovery = 91% Analysis Date = 07/01/15 Pct Recovery = 91% Analysis Date = 07/01/15 Pct Recovery = 91% Analysis Date = 06/26/15 Pct Recovery = 91% Analysis Date = 06/26/15 Pct Recovery = 91% Analysis Date = 06/21/15 Pct Recovery = 91% Analysis Date = 06/21/15 Pct Recovery = 91% Analysis Date = 06/17/15 Pct Recovery = 91% Analysis Date = 06/17/15 Pct Recovery = 91% Analysis Date = 06/12/15 Pct Recovery = 91% Analysis Date = 06/12/15 Pct Recovery = 91% Analysis Date = 06/07/15 Pct Recovery = 91% Analysis Date = 06/07/15 Pct Recovery = 91% Analysis Date = 06/02/15 Pct Recovery = 91% Analysis Date = 06/02/15 Pct Recovery = 91% Analysis Date = 05/29/15 Pct Recovery = 91% Analysis Date = 05/29/15 Pct Recovery = 91% Analysis Date = 05/24/15 Pct Recovery = 91% Analysis Date = 05/24/15 Pct Recovery = 91% Analysis Date = 05/19/15 Pct Recovery = 91% Analysis Date = 05/19/15 Pct Recovery = 91% Analysis Date = 05/14/15 Pct Recovery = 91% Analysis Date = 05/14/15 Pct Recovery = 91% Analysis Date = 05/10/15 Pct Recovery = 91% Analysis Date = 05/10/15 Pct Recovery = 91% Analysis Date = 05/05/15 Pct Recovery = 91% Analysis Date = 05/05/15 Pct Recovery = 91% Analysis Date = 04/30/15 Pct Recovery = 91% Analysis Date = 04/30/15 Pct Recovery = 91% Analysis Date = 04/25/15 Pct Recovery = 91% Analysis Date = 04/25/15 Pct Recovery = 91% Analysis Date = 04/20/15 Pct Recovery = 91% Analysis Date = 04/20/15 Pct Recovery = 91% Analysis Date = 04/16/15 Pct Recovery = 90% Analysis Date = 04/16/15 Pct Recovery = 90% Analysis Date = 04/11/15 Pct Recovery = 90% Analysis Date = 04/11/15 Pct Recovery = 90% Analysis Date = 04/06/15 Pct Recovery = 90% Analysis Date = 04/06/15 Pct Recovery = 90% Analysis Date = 04/01/15 Pct Recovery = 90% Analysis Date = 04/01/15 Pct Recovery = 90% Analysis Date = 03/28/15 Pct Recovery = 90% Analysis Date = 03/28/15 Pct Recovery = 90% Analysis Date = 03/23/15 Pct Recovery = 90% Analysis Date = 03/23/15 Pct Recovery = 90% Analysis Date = 03/18/15 Pct Recovery = 90% Analysis Date = 03/18/15 Pct Recovery = 90% Analysis Date = 03/13/15 Pct Recovery = 90% Analysis Date = 03/13/15 Pct Recovery = 90% Analysis Date = 03/09/15 Pct Recovery = 90% Analysis Date = 03/09/15 Pct Recovery = 90% Analysis Date = 03/04/15 Pct Recovery = 90% Analysis Date = 03/04/15 Pct Recovery = 90% Analysis Date = 02/27/15 Pct Recovery = 90% Analysis Date = 02/27/15 Pct Recovery = 90% Analysis Date = 02/22/15 Pct Recovery = 90% Analysis Date = 02/22/15 Pct Recovery = 90% Analysis Date = 02/17/15 Pct Recovery = 90% Analysis Date = 02/17/15 Pct Recovery = 90% Analysis Date = 02/13/15 Pct Recovery = 90% Analysis Date = 02/13/15 Pct Recovery = 90% Analysis Date = 02/08/15 Pct Recovery = 90% Analysis Date = 02/08/15 Pct Recovery = 90% Analysis Date = 02/03/15 Pct Recovery = 90% Analysis Date = 02/03/15 Pct Recovery = 90% Analysis Date = 01/29/15 Pct Recovery = 90% Analysis Date = 01/29/15 Pct Recovery = 90% Analysis Date = 01/25/15 Pct Recovery = 89% Analysis Date = 01/25/15 Pct Recovery = 89% Analysis Date = 01/20/15 Pct Recovery = 89% Analysis Date = 01/20/15 Pct Recovery = 89% Analysis Date = 01/15/15 Pct Recovery = 89% Analysis Date = 01/15/15 Pct Recovery = 89% Analysis Date = 01/10/15 Pct Recovery = 89% Analysis Date = 01/10/15 Pct Recovery = 89% Analysis Date = 01/06/15 Pct Recovery = 89% Analysis Date = 01/06/15 Pct Recovery = 89% Analysis Date = 01/01/15 Pct Recovery = 89% Analysis Date = 01/01/15 Pct Recovery = 89% Analysis Date = 12/27/14 Pct Recovery = 89% Analysis Date = 12/27/14 Pct Recovery = 89% Analysis Date = 12/22/14 Pct Recovery = 89% Analysis Date = 12/22/14 Pct Recovery = 89% Analysis Date = 12/17/14 Pct Recovery = 89% Analysis Date = 12/17/14 Pct Recovery = 89% Analysis Date = 12/13/14 Pct Recovery = 89% Analysis Date = 12/13/14 Pct Recovery = 89% Analysis Date = 12/08/14 Pct Recovery = 89% Analysis Date = 12/08/14 Pct Recovery = 89% Analysis Date = 12/03/14 Pct Recovery = 88% Analysis Date = 12/03/14 Pct Recovery = 88% Analysis Date = 11/28/14 Pct Recovery = 88% Analysis Date = 11/28/14 Pct Recovery = 88% Analysis Date = 11/24/14 Pct Recovery = 88% Analysis Date = 11/24/14 Pct Recovery = 88% Analysis Date = 11/19/14 Pct Recovery = 88% Analysis Date = 11/19/14 Pct Recovery = 88% Analysis Date = 11/14/14 Pct Recovery = 88% Analysis Date = 11/14/14 Pct Recovery = 88% Analysis Date = 11/09/14 Pct Recovery = 88% Analysis Date = 11/09/14 Pct Recovery = 88% Analysis Date = 11/05/14 Pct Recovery = 88% Analysis Date = 11/05/14 Pct Recovery = 88% Analysis Date = 10/31/14 Pct Recovery = 88% Analysis Date = 10/31/14 Pct Recovery = 88% Analysis Date = 10/26/14 Pct Recovery = 88% Analysis Date = 10/26/14 Pct Recovery = 88% Analysis Date = 10/21/14 Pct Recovery = 88% Analysis Date = 10/21/14 Pct Recovery = 88% Analysis Date = 10/16/14 Pct Recovery = 87% Analysis Date = 10/16/14 Pct Recovery = 87% Analysis Date = 10/12/14 Pct Recovery = 87% Analysis Date = 10/12/14 Pct Recovery = 87% Analysis Date = 10/07/14 Pct Recovery = 87% Analysis Date = 10/07/14 Pct Recovery = 87% Analysis Date = 10/02/14 Pct Recovery = 87% Analysis Date = 10/02/14 Pct Recovery = 87% Analysis Date = 09/27/14 Pct Recovery = 87% Analysis Date = 09/27/14 Pct Recovery = 87% Analysis Date = 09/23/14 Pct Recovery = 87% Analysis Date = 09/23/14 Pct Recovery = 87% Analysis Date = 09/18/14 Pct Recovery = 87% Analysis Date = 09/18/14 Pct Recovery = 87% Analysis Date = 09/13/14 Pct Recovery = 87% Analysis Date = 09/13/14 Pct Recovery = 87% Analysis Date = 09/08/14 Pct Recovery = 86% Analysis Date = 09/08/14 Pct Recovery = 86% Analysis Date = 09/04/14 Pct Recovery = 86% Analysis Date = 09/04/14 Pct Recovery = 86% Analysis Date = 08/30/14 Pct Recovery = 86% Analysis Date = 08/30/14 Pct Recovery = 86% Analysis Date = 08/25/14 Pct Recovery = 86% Analysis Date = 08/25/14 Pct Recovery = 86% Analysis Date = 08/20/14 Pct Recovery = 86% Analysis Date = 08/20/14 Pct Recovery = 86% Analysis Date = 08/15/14 Pct Recovery = 86% Analysis Date = 08/15/14 Pct Recovery = 86% Analysis Date = 08/11/14 Pct Recovery = 86% Analysis Date = 08/11/14 Pct Recovery = 86% Analysis Date = 08/06/14 Pct Recovery = 86% Analysis Date = 08/06/14 Pct Recovery = 86% Analysis Date = 08/01/14 Pct Recovery = 86% Analysis Date = 08/01/14 Pct Recovery = 86% Analysis Date = 07/27/14 Pct Recovery = 85% Analysis Date = 07/27/14 Pct Recovery = 85% Analysis Date = 07/23/14 Pct Recovery = 85% Analysis Date = 07/23/14 Pct Recovery = 85% Analysis Date = 07/18/14 Pct Recovery = 85% Analysis Date = 07/18/14 Pct Recovery = 85% Analysis Date = 07/13/14 Pct Recovery = 85% Analysis Date = 07/13/14 Pct Recovery = 85% Analysis Date = 07/08/14 Pct Recovery = 85% Analysis Date = 07/08/14 Pct Recovery = 85% Analysis Date = 07/04/14 Pct Recovery = 85% Analysis Date = 07/04/14 Pct Recovery = 85% Analysis Date = 06/29/14 Pct Recovery = 85% Analysis Date = 06/29/14 Pct Recovery = 85% Analysis Date = 06/24/14 Pct Recovery = 85% Analysis Date = 06/24/14 Pct Recovery = 85% Analysis Date = 06/19/14 Pct Recovery = 84% Analysis Date = 06/19/14 Pct Recovery = 84% Analysis Date = 06/14/14 Pct Recovery = 84% Analysis Date = 06/14/14 Pct Recovery = 84% Analysis Date = 06/10/14 Pct Recovery = 84% Analysis Date = 06/10/14 Pct Recovery = 84% Analysis Date = 06/05/14 Pct Recovery = 84% Analysis Date = 06/05/14 Pct Recovery = 84% Analysis Date = 05/31/14 Pct Recovery = 84% Analysis Date = 05/31/14 Pct Recovery = 84% Analysis Date = 05/26/14 Pct Recovery = 84% Analysis Date = 05/26/14 Pct Recovery = 84% Analysis Date = 05/22/14 Pct Recovery = 84% Analysis Date = 05/22/14 Pct Recovery = 84% Analysis Date = 05/17/14 Pct Recovery = 84% Analysis Date = 05/17/14 Pct Recovery = 84% Analysis Date = 05/12/14 Pct Recovery = 84% Analysis Date = 05/12/14 Pct Recovery = 84% Analysis Date = 05/07/14 Pct Recovery = 83% Analysis Date = 05/07/14 Pct Recovery = 83% Analysis Date = 05/03/14 Pct Recovery = 83% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
1,2,4-TRICHLOROBENZENE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 48 87% 9% 88% 9%
Total 48 87% 9% 88% 9%

Sample Statistics
1,2,4-TRICHLOROBENZENE

Characteristic N % % Basis
Plotted 48 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 48 .  
False Negatives 0 0% 0 out of 48
Not Spiked 25 .  
False Positives 0 0% 0 out of 25

BQS OBSP Determination:
1,2,4-TRIMETHYLBENZENE
METHOD: 4440 , TESTIDCODE: 77222GCM66
Open Data Set

Analysis Date = 12/12/16 SpikeMix = Accu 216041125: 40 µl & Crescent 03FF058: 40 µl Pct Recovery = 110% Analysis Date = 07/20/16 SpikeMix = Supelco LC20141V: 40 µl & Accu 216041125: 40 µl Pct Recovery = 99% Analysis Date = 07/14/16 SpikeMix = Accu 216041125: 40 µl & NSI 041816AVOC: 40 µl Pct Recovery = 87% Analysis Date = 09/08/16 SpikeMix = Supelco LC20141V: 25 µl & Accu 216041125: 25 µl Pct Recovery = 76% Analysis Date = 05/24/16 SpikeMix = Accu 216041125: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 94% Analysis Date = 08/12/16 SpikeMix = ChemService 5082900: 25 µl & Phenova B20160319: 25 µl Pct Recovery = 90% Analysis Date = 06/21/16 SpikeMix = Phenova B20160319: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 105% Analysis Date = 03/19/15 SpikeMix = Spex Organics C1140417015: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 96% Analysis Date = 03/06/15 SpikeMix = ERA 0227-14-06.1A: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 77% Analysis Date = 12/17/14 SpikeMix = Supelco LC06438: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 86% Analysis Date = 11/22/14 SpikeMix = NSI 032614: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 87% Analysis Date = 09/21/14 SpikeMix = Supelco LC06438: 20 µl Pct Recovery = 74% Analysis Date = 08/19/14 SpikeMix = Spex Organics C1140417015: 20 µl & Accu 214031115: 20 µl Pct Recovery = 90% Analysis Date = 08/16/14 SpikeMix = ERA 0227-14-06.1A: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 84% Analysis Date = 06/10/14 SpikeMix = NSI 032614: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 80% Analysis Date = 09/29/15 SpikeMix = Accu 215041380: 25 µl & ERA 0406-15-03: 25 µl Pct Recovery = 76% Analysis Date = 08/15/15 SpikeMix = Supelco LC13545: 25 µl & Crescent 04EE008: 25 µl Pct Recovery = 104% Analysis Date = 07/13/15 SpikeMix = Crescent 04EE008: 25 µl & NSI 050515AVOC: 25 µl Pct Recovery = 86% Analysis Date = 10/13/16 SpikeMix = Accu 216041125: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 90% Analysis Date = 08/20/16 SpikeMix = Accu 216041125: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 98% Analysis Date = 06/30/16 SpikeMix = ChemService 5082900: 15 µl & Accu 216041125: 15 µl Pct Recovery = 65% Analysis Date = 11/29/16 SpikeMix = ChemService 5082900: 15 µl & Phenova B20160319: 15 µl Pct Recovery = 87% Analysis Date = 09/08/16 SpikeMix = Phenova B20160319: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 83% Analysis Date = 07/29/16 SpikeMix = Phenova B20160319: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 92% Analysis Date = 05/27/16 SpikeMix = Phenova B20160319: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 90% Analysis Date = 04/02/16 SpikeMix = Supelco LC13545: 15 µl & Accu 215041380: 15 µl Pct Recovery = 79% Analysis Date = 03/04/16 SpikeMix = Accu 215041380: 15 µl & ERA 0406-15-03: 15 µl Pct Recovery = 71% Analysis Date = 06/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Accu 215041380: 15 µl Pct Recovery = 76% Analysis Date = 12/18/15 SpikeMix = Supelco LC13545: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 104% Analysis Date = 10/17/15 SpikeMix = Crescent 04EE008: 15 µl & NSI 050515AVOC: 15 µl Pct Recovery = 105% Analysis Date = 05/09/15 SpikeMix = Spex Organics EN150428007: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 104% Analysis Date = 11/06/14 SpikeMix = Spex Organics C1140417015: 10 µl & Crescent 03DD004: 10 µl Pct Recovery = 96% Analysis Date = 10/21/14 SpikeMix = ERA 0227-14-06.1A: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 86% Analysis Date = 09/09/14 SpikeMix = NSI 032614: 10 µl & Spex Organics C1140417015: 10 µl Pct Recovery = 104% Analysis Date = 07/23/14 SpikeMix = Spex Organics C1140417015: 10 µl & Accu 214031115: 10 µl Pct Recovery = 93% Analysis Date = 07/11/14 SpikeMix = Spex Organics C1140417015: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 88% Analysis Date = 06/18/14 SpikeMix = Supelco LC06438: 10 µl & Accu 214031115: 10 µl Pct Recovery = 80% Analysis Date = 05/30/14 SpikeMix = NSI 032614: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 72% Analysis Date = 05/03/14 SpikeMix = Crescent 03DD004: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 92% Analysis Date = 02/18/16 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 85% Analysis Date = 11/20/15 SpikeMix = Accu 215041380: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 91% Analysis Date = 11/12/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 108% Analysis Date = 05/21/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 100% Analysis Date = 05/13/16 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 100% Analysis Date = 01/27/16 SpikeMix = Crescent 04EE008: 10 µl & NSI 050515AVOC: 10 µl Pct Recovery = 102% Analysis Date = 08/07/15 SpikeMix = Crescent 04EE008: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 94% Analysis Date = 05/09/15 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 104% Analysis Date = 12/12/16 Pct Recovery = 91% Analysis Date = 12/07/16 Pct Recovery = 91% Analysis Date = 12/07/16 Pct Recovery = 91% Analysis Date = 12/02/16 Pct Recovery = 91% Analysis Date = 12/02/16 Pct Recovery = 91% Analysis Date = 11/27/16 Pct Recovery = 91% Analysis Date = 11/27/16 Pct Recovery = 91% Analysis Date = 11/22/16 Pct Recovery = 91% Analysis Date = 11/22/16 Pct Recovery = 91% Analysis Date = 11/18/16 Pct Recovery = 91% Analysis Date = 11/18/16 Pct Recovery = 91% Analysis Date = 11/13/16 Pct Recovery = 91% Analysis Date = 11/13/16 Pct Recovery = 91% Analysis Date = 11/08/16 Pct Recovery = 91% Analysis Date = 11/08/16 Pct Recovery = 91% Analysis Date = 11/03/16 Pct Recovery = 91% Analysis Date = 11/03/16 Pct Recovery = 91% Analysis Date = 10/30/16 Pct Recovery = 91% Analysis Date = 10/30/16 Pct Recovery = 91% Analysis Date = 10/25/16 Pct Recovery = 91% Analysis Date = 10/25/16 Pct Recovery = 91% Analysis Date = 10/20/16 Pct Recovery = 91% Analysis Date = 10/20/16 Pct Recovery = 91% Analysis Date = 10/15/16 Pct Recovery = 91% Analysis Date = 10/15/16 Pct Recovery = 91% Analysis Date = 10/10/16 Pct Recovery = 91% Analysis Date = 10/10/16 Pct Recovery = 91% Analysis Date = 10/06/16 Pct Recovery = 91% Analysis Date = 10/06/16 Pct Recovery = 91% Analysis Date = 10/01/16 Pct Recovery = 91% Analysis Date = 10/01/16 Pct Recovery = 91% Analysis Date = 09/26/16 Pct Recovery = 91% Analysis Date = 09/26/16 Pct Recovery = 91% Analysis Date = 09/21/16 Pct Recovery = 91% Analysis Date = 09/21/16 Pct Recovery = 91% Analysis Date = 09/17/16 Pct Recovery = 91% Analysis Date = 09/17/16 Pct Recovery = 91% Analysis Date = 09/12/16 Pct Recovery = 91% Analysis Date = 09/12/16 Pct Recovery = 91% Analysis Date = 09/07/16 Pct Recovery = 91% Analysis Date = 09/07/16 Pct Recovery = 91% Analysis Date = 09/02/16 Pct Recovery = 91% Analysis Date = 09/02/16 Pct Recovery = 91% Analysis Date = 08/29/16 Pct Recovery = 90% Analysis Date = 08/29/16 Pct Recovery = 90% Analysis Date = 08/24/16 Pct Recovery = 90% Analysis Date = 08/24/16 Pct Recovery = 90% Analysis Date = 08/19/16 Pct Recovery = 90% Analysis Date = 08/19/16 Pct Recovery = 90% Analysis Date = 08/14/16 Pct Recovery = 90% Analysis Date = 08/14/16 Pct Recovery = 90% Analysis Date = 08/09/16 Pct Recovery = 90% Analysis Date = 08/09/16 Pct Recovery = 90% Analysis Date = 08/05/16 Pct Recovery = 90% Analysis Date = 08/05/16 Pct Recovery = 90% Analysis Date = 07/31/16 Pct Recovery = 90% Analysis Date = 07/31/16 Pct Recovery = 90% Analysis Date = 07/26/16 Pct Recovery = 90% Analysis Date = 07/26/16 Pct Recovery = 90% Analysis Date = 07/21/16 Pct Recovery = 90% Analysis Date = 07/21/16 Pct Recovery = 90% Analysis Date = 07/17/16 Pct Recovery = 90% Analysis Date = 07/17/16 Pct Recovery = 90% Analysis Date = 07/12/16 Pct Recovery = 90% Analysis Date = 07/12/16 Pct Recovery = 90% Analysis Date = 07/07/16 Pct Recovery = 90% Analysis Date = 07/07/16 Pct Recovery = 90% Analysis Date = 07/02/16 Pct Recovery = 90% Analysis Date = 07/02/16 Pct Recovery = 90% Analysis Date = 06/28/16 Pct Recovery = 90% Analysis Date = 06/28/16 Pct Recovery = 90% Analysis Date = 06/23/16 Pct Recovery = 90% Analysis Date = 06/23/16 Pct Recovery = 90% Analysis Date = 06/18/16 Pct Recovery = 90% Analysis Date = 06/18/16 Pct Recovery = 90% Analysis Date = 06/13/16 Pct Recovery = 91% Analysis Date = 06/13/16 Pct Recovery = 91% Analysis Date = 06/08/16 Pct Recovery = 91% Analysis Date = 06/08/16 Pct Recovery = 91% Analysis Date = 06/04/16 Pct Recovery = 91% Analysis Date = 06/04/16 Pct Recovery = 91% Analysis Date = 05/30/16 Pct Recovery = 91% Analysis Date = 05/30/16 Pct Recovery = 91% Analysis Date = 05/25/16 Pct Recovery = 91% Analysis Date = 05/25/16 Pct Recovery = 91% Analysis Date = 05/20/16 Pct Recovery = 91% Analysis Date = 05/20/16 Pct Recovery = 91% Analysis Date = 05/16/16 Pct Recovery = 91% Analysis Date = 05/16/16 Pct Recovery = 91% Analysis Date = 05/11/16 Pct Recovery = 91% Analysis Date = 05/11/16 Pct Recovery = 91% Analysis Date = 05/06/16 Pct Recovery = 91% Analysis Date = 05/06/16 Pct Recovery = 91% Analysis Date = 05/01/16 Pct Recovery = 91% Analysis Date = 05/01/16 Pct Recovery = 91% Analysis Date = 04/27/16 Pct Recovery = 91% Analysis Date = 04/27/16 Pct Recovery = 91% Analysis Date = 04/22/16 Pct Recovery = 91% Analysis Date = 04/22/16 Pct Recovery = 91% Analysis Date = 04/17/16 Pct Recovery = 91% Analysis Date = 04/17/16 Pct Recovery = 91% Analysis Date = 04/12/16 Pct Recovery = 91% Analysis Date = 04/12/16 Pct Recovery = 91% Analysis Date = 04/07/16 Pct Recovery = 91% Analysis Date = 04/07/16 Pct Recovery = 91% Analysis Date = 04/03/16 Pct Recovery = 91% Analysis Date = 04/03/16 Pct Recovery = 91% Analysis Date = 03/29/16 Pct Recovery = 91% Analysis Date = 03/29/16 Pct Recovery = 91% Analysis Date = 03/24/16 Pct Recovery = 91% Analysis Date = 03/24/16 Pct Recovery = 91% Analysis Date = 03/19/16 Pct Recovery = 92% Analysis Date = 03/19/16 Pct Recovery = 92% Analysis Date = 03/15/16 Pct Recovery = 92% Analysis Date = 03/15/16 Pct Recovery = 92% Analysis Date = 03/10/16 Pct Recovery = 92% Analysis Date = 03/10/16 Pct Recovery = 92% Analysis Date = 03/05/16 Pct Recovery = 92% Analysis Date = 03/05/16 Pct Recovery = 92% Analysis Date = 02/29/16 Pct Recovery = 92% Analysis Date = 02/29/16 Pct Recovery = 92% Analysis Date = 02/25/16 Pct Recovery = 92% Analysis Date = 02/25/16 Pct Recovery = 92% Analysis Date = 02/20/16 Pct Recovery = 92% Analysis Date = 02/20/16 Pct Recovery = 92% Analysis Date = 02/15/16 Pct Recovery = 92% Analysis Date = 02/15/16 Pct Recovery = 92% Analysis Date = 02/10/16 Pct Recovery = 92% Analysis Date = 02/10/16 Pct Recovery = 92% Analysis Date = 02/05/16 Pct Recovery = 92% Analysis Date = 02/05/16 Pct Recovery = 92% Analysis Date = 02/01/16 Pct Recovery = 92% Analysis Date = 02/01/16 Pct Recovery = 92% Analysis Date = 01/27/16 Pct Recovery = 92% Analysis Date = 01/27/16 Pct Recovery = 92% Analysis Date = 01/22/16 Pct Recovery = 92% Analysis Date = 01/22/16 Pct Recovery = 92% Analysis Date = 01/17/16 Pct Recovery = 92% Analysis Date = 01/17/16 Pct Recovery = 92% Analysis Date = 01/13/16 Pct Recovery = 92% Analysis Date = 01/13/16 Pct Recovery = 92% Analysis Date = 01/08/16 Pct Recovery = 92% Analysis Date = 01/08/16 Pct Recovery = 92% Analysis Date = 01/03/16 Pct Recovery = 92% Analysis Date = 01/03/16 Pct Recovery = 92% Analysis Date = 12/29/15 Pct Recovery = 93% Analysis Date = 12/29/15 Pct Recovery = 93% Analysis Date = 12/25/15 Pct Recovery = 93% Analysis Date = 12/25/15 Pct Recovery = 93% Analysis Date = 12/20/15 Pct Recovery = 93% Analysis Date = 12/20/15 Pct Recovery = 93% Analysis Date = 12/15/15 Pct Recovery = 93% Analysis Date = 12/15/15 Pct Recovery = 93% Analysis Date = 12/10/15 Pct Recovery = 93% Analysis Date = 12/10/15 Pct Recovery = 93% Analysis Date = 12/05/15 Pct Recovery = 93% Analysis Date = 12/05/15 Pct Recovery = 93% Analysis Date = 12/01/15 Pct Recovery = 93% Analysis Date = 12/01/15 Pct Recovery = 93% Analysis Date = 11/26/15 Pct Recovery = 93% Analysis Date = 11/26/15 Pct Recovery = 93% Analysis Date = 11/21/15 Pct Recovery = 93% Analysis Date = 11/21/15 Pct Recovery = 93% Analysis Date = 11/16/15 Pct Recovery = 93% Analysis Date = 11/16/15 Pct Recovery = 93% Analysis Date = 11/12/15 Pct Recovery = 93% Analysis Date = 11/12/15 Pct Recovery = 93% Analysis Date = 11/07/15 Pct Recovery = 93% Analysis Date = 11/07/15 Pct Recovery = 93% Analysis Date = 11/02/15 Pct Recovery = 93% Analysis Date = 11/02/15 Pct Recovery = 93% Analysis Date = 10/28/15 Pct Recovery = 93% Analysis Date = 10/28/15 Pct Recovery = 93% Analysis Date = 10/24/15 Pct Recovery = 93% Analysis Date = 10/24/15 Pct Recovery = 93% Analysis Date = 10/19/15 Pct Recovery = 93% Analysis Date = 10/19/15 Pct Recovery = 93% Analysis Date = 10/14/15 Pct Recovery = 93% Analysis Date = 10/14/15 Pct Recovery = 93% Analysis Date = 10/09/15 Pct Recovery = 93% Analysis Date = 10/09/15 Pct Recovery = 93% Analysis Date = 10/04/15 Pct Recovery = 93% Analysis Date = 10/04/15 Pct Recovery = 93% Analysis Date = 09/30/15 Pct Recovery = 93% Analysis Date = 09/30/15 Pct Recovery = 93% Analysis Date = 09/25/15 Pct Recovery = 93% Analysis Date = 09/25/15 Pct Recovery = 93% Analysis Date = 09/20/15 Pct Recovery = 93% Analysis Date = 09/20/15 Pct Recovery = 93% Analysis Date = 09/15/15 Pct Recovery = 93% Analysis Date = 09/15/15 Pct Recovery = 93% Analysis Date = 09/11/15 Pct Recovery = 93% Analysis Date = 09/11/15 Pct Recovery = 93% Analysis Date = 09/06/15 Pct Recovery = 93% Analysis Date = 09/06/15 Pct Recovery = 93% Analysis Date = 09/01/15 Pct Recovery = 93% Analysis Date = 09/01/15 Pct Recovery = 93% Analysis Date = 08/27/15 Pct Recovery = 93% Analysis Date = 08/27/15 Pct Recovery = 93% Analysis Date = 08/23/15 Pct Recovery = 93% Analysis Date = 08/23/15 Pct Recovery = 93% Analysis Date = 08/18/15 Pct Recovery = 93% Analysis Date = 08/18/15 Pct Recovery = 93% Analysis Date = 08/13/15 Pct Recovery = 93% Analysis Date = 08/13/15 Pct Recovery = 93% Analysis Date = 08/08/15 Pct Recovery = 93% Analysis Date = 08/08/15 Pct Recovery = 93% Analysis Date = 08/03/15 Pct Recovery = 93% Analysis Date = 08/03/15 Pct Recovery = 93% Analysis Date = 07/30/15 Pct Recovery = 93% Analysis Date = 07/30/15 Pct Recovery = 93% Analysis Date = 07/25/15 Pct Recovery = 93% Analysis Date = 07/25/15 Pct Recovery = 93% Analysis Date = 07/20/15 Pct Recovery = 93% Analysis Date = 07/20/15 Pct Recovery = 93% Analysis Date = 07/15/15 Pct Recovery = 93% Analysis Date = 07/15/15 Pct Recovery = 93% Analysis Date = 07/11/15 Pct Recovery = 93% Analysis Date = 07/11/15 Pct Recovery = 93% Analysis Date = 07/06/15 Pct Recovery = 93% Analysis Date = 07/06/15 Pct Recovery = 93% Analysis Date = 07/01/15 Pct Recovery = 93% Analysis Date = 07/01/15 Pct Recovery = 93% Analysis Date = 06/26/15 Pct Recovery = 93% Analysis Date = 06/26/15 Pct Recovery = 93% Analysis Date = 06/21/15 Pct Recovery = 93% Analysis Date = 06/21/15 Pct Recovery = 93% Analysis Date = 06/17/15 Pct Recovery = 93% Analysis Date = 06/17/15 Pct Recovery = 93% Analysis Date = 06/12/15 Pct Recovery = 93% Analysis Date = 06/12/15 Pct Recovery = 93% Analysis Date = 06/07/15 Pct Recovery = 93% Analysis Date = 06/07/15 Pct Recovery = 93% Analysis Date = 06/02/15 Pct Recovery = 93% Analysis Date = 06/02/15 Pct Recovery = 93% Analysis Date = 05/29/15 Pct Recovery = 93% Analysis Date = 05/29/15 Pct Recovery = 93% Analysis Date = 05/24/15 Pct Recovery = 93% Analysis Date = 05/24/15 Pct Recovery = 93% Analysis Date = 05/19/15 Pct Recovery = 93% Analysis Date = 05/19/15 Pct Recovery = 93% Analysis Date = 05/14/15 Pct Recovery = 92% Analysis Date = 05/14/15 Pct Recovery = 92% Analysis Date = 05/10/15 Pct Recovery = 92% Analysis Date = 05/10/15 Pct Recovery = 92% Analysis Date = 05/05/15 Pct Recovery = 92% Analysis Date = 05/05/15 Pct Recovery = 92% Analysis Date = 04/30/15 Pct Recovery = 92% Analysis Date = 04/30/15 Pct Recovery = 92% Analysis Date = 04/25/15 Pct Recovery = 92% Analysis Date = 04/25/15 Pct Recovery = 92% Analysis Date = 04/20/15 Pct Recovery = 92% Analysis Date = 04/20/15 Pct Recovery = 92% Analysis Date = 04/16/15 Pct Recovery = 92% Analysis Date = 04/16/15 Pct Recovery = 92% Analysis Date = 04/11/15 Pct Recovery = 92% Analysis Date = 04/11/15 Pct Recovery = 92% Analysis Date = 04/06/15 Pct Recovery = 92% Analysis Date = 04/06/15 Pct Recovery = 92% Analysis Date = 04/01/15 Pct Recovery = 92% Analysis Date = 04/01/15 Pct Recovery = 92% Analysis Date = 03/28/15 Pct Recovery = 92% Analysis Date = 03/28/15 Pct Recovery = 92% Analysis Date = 03/23/15 Pct Recovery = 91% Analysis Date = 03/23/15 Pct Recovery = 91% Analysis Date = 03/18/15 Pct Recovery = 91% Analysis Date = 03/18/15 Pct Recovery = 91% Analysis Date = 03/13/15 Pct Recovery = 91% Analysis Date = 03/13/15 Pct Recovery = 91% Analysis Date = 03/09/15 Pct Recovery = 91% Analysis Date = 03/09/15 Pct Recovery = 91% Analysis Date = 03/04/15 Pct Recovery = 91% Analysis Date = 03/04/15 Pct Recovery = 91% Analysis Date = 02/27/15 Pct Recovery = 91% Analysis Date = 02/27/15 Pct Recovery = 91% Analysis Date = 02/22/15 Pct Recovery = 91% Analysis Date = 02/22/15 Pct Recovery = 91% Analysis Date = 02/17/15 Pct Recovery = 91% Analysis Date = 02/17/15 Pct Recovery = 91% Analysis Date = 02/13/15 Pct Recovery = 91% Analysis Date = 02/13/15 Pct Recovery = 91% Analysis Date = 02/08/15 Pct Recovery = 90% Analysis Date = 02/08/15 Pct Recovery = 90% Analysis Date = 02/03/15 Pct Recovery = 90% Analysis Date = 02/03/15 Pct Recovery = 90% Analysis Date = 01/29/15 Pct Recovery = 90% Analysis Date = 01/29/15 Pct Recovery = 90% Analysis Date = 01/25/15 Pct Recovery = 90% Analysis Date = 01/25/15 Pct Recovery = 90% Analysis Date = 01/20/15 Pct Recovery = 90% Analysis Date = 01/20/15 Pct Recovery = 90% Analysis Date = 01/15/15 Pct Recovery = 90% Analysis Date = 01/15/15 Pct Recovery = 90% Analysis Date = 01/10/15 Pct Recovery = 90% Analysis Date = 01/10/15 Pct Recovery = 90% Analysis Date = 01/06/15 Pct Recovery = 90% Analysis Date = 01/06/15 Pct Recovery = 90% Analysis Date = 01/01/15 Pct Recovery = 90% Analysis Date = 01/01/15 Pct Recovery = 90% Analysis Date = 12/27/14 Pct Recovery = 89% Analysis Date = 12/27/14 Pct Recovery = 89% Analysis Date = 12/22/14 Pct Recovery = 89% Analysis Date = 12/22/14 Pct Recovery = 89% Analysis Date = 12/17/14 Pct Recovery = 89% Analysis Date = 12/17/14 Pct Recovery = 89% Analysis Date = 12/13/14 Pct Recovery = 89% Analysis Date = 12/13/14 Pct Recovery = 89% Analysis Date = 12/08/14 Pct Recovery = 89% Analysis Date = 12/08/14 Pct Recovery = 89% Analysis Date = 12/03/14 Pct Recovery = 89% Analysis Date = 12/03/14 Pct Recovery = 89% Analysis Date = 11/28/14 Pct Recovery = 89% Analysis Date = 11/28/14 Pct Recovery = 89% Analysis Date = 11/24/14 Pct Recovery = 89% Analysis Date = 11/24/14 Pct Recovery = 89% Analysis Date = 11/19/14 Pct Recovery = 89% Analysis Date = 11/19/14 Pct Recovery = 89% Analysis Date = 11/14/14 Pct Recovery = 88% Analysis Date = 11/14/14 Pct Recovery = 88% Analysis Date = 11/09/14 Pct Recovery = 88% Analysis Date = 11/09/14 Pct Recovery = 88% Analysis Date = 11/05/14 Pct Recovery = 88% Analysis Date = 11/05/14 Pct Recovery = 88% Analysis Date = 10/31/14 Pct Recovery = 88% Analysis Date = 10/31/14 Pct Recovery = 88% Analysis Date = 10/26/14 Pct Recovery = 88% Analysis Date = 10/26/14 Pct Recovery = 88% Analysis Date = 10/21/14 Pct Recovery = 88% Analysis Date = 10/21/14 Pct Recovery = 88% Analysis Date = 10/16/14 Pct Recovery = 88% Analysis Date = 10/16/14 Pct Recovery = 88% Analysis Date = 10/12/14 Pct Recovery = 88% Analysis Date = 10/12/14 Pct Recovery = 88% Analysis Date = 10/07/14 Pct Recovery = 87% Analysis Date = 10/07/14 Pct Recovery = 87% Analysis Date = 10/02/14 Pct Recovery = 87% Analysis Date = 10/02/14 Pct Recovery = 87% Analysis Date = 09/27/14 Pct Recovery = 87% Analysis Date = 09/27/14 Pct Recovery = 87% Analysis Date = 09/23/14 Pct Recovery = 87% Analysis Date = 09/23/14 Pct Recovery = 87% Analysis Date = 09/18/14 Pct Recovery = 87% Analysis Date = 09/18/14 Pct Recovery = 87% Analysis Date = 09/13/14 Pct Recovery = 87% Analysis Date = 09/13/14 Pct Recovery = 87% Analysis Date = 09/08/14 Pct Recovery = 87% Analysis Date = 09/08/14 Pct Recovery = 87% Analysis Date = 09/04/14 Pct Recovery = 87% Analysis Date = 09/04/14 Pct Recovery = 87% Analysis Date = 08/30/14 Pct Recovery = 87% Analysis Date = 08/30/14 Pct Recovery = 87% Analysis Date = 08/25/14 Pct Recovery = 86% Analysis Date = 08/25/14 Pct Recovery = 86% Analysis Date = 08/20/14 Pct Recovery = 86% Analysis Date = 08/20/14 Pct Recovery = 86% Analysis Date = 08/15/14 Pct Recovery = 86% Analysis Date = 08/15/14 Pct Recovery = 86% Analysis Date = 08/11/14 Pct Recovery = 86% Analysis Date = 08/11/14 Pct Recovery = 86% Analysis Date = 08/06/14 Pct Recovery = 86% Analysis Date = 08/06/14 Pct Recovery = 86% Analysis Date = 08/01/14 Pct Recovery = 86% Analysis Date = 08/01/14 Pct Recovery = 86% Analysis Date = 07/27/14 Pct Recovery = 86% Analysis Date = 07/27/14 Pct Recovery = 86% Analysis Date = 07/23/14 Pct Recovery = 86% Analysis Date = 07/23/14 Pct Recovery = 86% Analysis Date = 07/18/14 Pct Recovery = 86% Analysis Date = 07/18/14 Pct Recovery = 86% Analysis Date = 07/13/14 Pct Recovery = 85% Analysis Date = 07/13/14 Pct Recovery = 85% Analysis Date = 07/08/14 Pct Recovery = 85% Analysis Date = 07/08/14 Pct Recovery = 85% Analysis Date = 07/04/14 Pct Recovery = 85% Analysis Date = 07/04/14 Pct Recovery = 85% Analysis Date = 06/29/14 Pct Recovery = 85% Analysis Date = 06/29/14 Pct Recovery = 85% Analysis Date = 06/24/14 Pct Recovery = 85% Analysis Date = 06/24/14 Pct Recovery = 85% Analysis Date = 06/19/14 Pct Recovery = 85% Analysis Date = 06/19/14 Pct Recovery = 85% Analysis Date = 06/14/14 Pct Recovery = 85% Analysis Date = 06/14/14 Pct Recovery = 85% Analysis Date = 06/10/14 Pct Recovery = 85% Analysis Date = 06/10/14 Pct Recovery = 85% Analysis Date = 06/05/14 Pct Recovery = 84% Analysis Date = 06/05/14 Pct Recovery = 84% Analysis Date = 05/31/14 Pct Recovery = 84% Analysis Date = 05/31/14 Pct Recovery = 84% Analysis Date = 05/26/14 Pct Recovery = 84% Analysis Date = 05/26/14 Pct Recovery = 84% Analysis Date = 05/22/14 Pct Recovery = 84% Analysis Date = 05/22/14 Pct Recovery = 84% Analysis Date = 05/17/14 Pct Recovery = 84% Analysis Date = 05/17/14 Pct Recovery = 84% Analysis Date = 05/12/14 Pct Recovery = 84% Analysis Date = 05/12/14 Pct Recovery = 84% Analysis Date = 05/07/14 Pct Recovery = 84% Analysis Date = 05/07/14 Pct Recovery = 84% Analysis Date = 05/03/14 Pct Recovery = 84% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
1,2,4-TRIMETHYLBENZENE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 47 90% 11% 90% 12%
Total 47 90% 11% 90% 12%

Sample Statistics
1,2,4-TRIMETHYLBENZENE

Characteristic N % % Basis
Plotted 47 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 47 .  
False Negatives 0 0% 0 out of 47
Not Spiked 26 .  
False Positives 0 0% 0 out of 26

BQS OBSP Determination:
1,2-DIBROMO-3-CHLOROPROPANE
METHOD: 4440 , TESTIDCODE: 82625GCM66
Open Data Set

Analysis Date = 12/16/16 SpikeMix = NSI 041816AVOC: 40 µl & ChemService 5082900: 40 µl Pct Recovery = 85% Analysis Date = 07/14/16 SpikeMix = Accu 216041125: 40 µl & NSI 041816AVOC: 40 µl Pct Recovery = 96% Analysis Date = 12/12/16 SpikeMix = Accu 216041125: 40 µl & Crescent 03FF058: 40 µl Pct Recovery = 86% Analysis Date = 08/04/16 SpikeMix = Crescent 03FF058: 40 µl & Supelco LC20141V: 40 µl Pct Recovery = 78% Analysis Date = 08/26/16 SpikeMix = NSI 041816AVOC: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 86% Analysis Date = 11/21/16 SpikeMix = Crescent 03FF058: 25 µl & Supelco LC20141V: 25 µl Pct Recovery = 87% Analysis Date = 06/30/16 SpikeMix = Crescent 03FF058: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 87% Analysis Date = 06/21/16 SpikeMix = Phenova B20160319: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 86% Analysis Date = 05/24/16 SpikeMix = Accu 216041125: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 79% Analysis Date = 07/13/15 SpikeMix = Crescent 04EE008: 25 µl & NSI 050515AVOC: 25 µl Pct Recovery = 69% Analysis Date = 09/29/15 SpikeMix = Accu 215041380: 25 µl & ERA 0406-15-03: 25 µl Pct Recovery = 80% Analysis Date = 06/16/15 SpikeMix = ERA 0406-15-03: 25 µl & Supelco LC13545: 25 µl Pct Recovery = 74% Analysis Date = 10/13/16 SpikeMix = Accu 216041125: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 79% Analysis Date = 10/13/16 SpikeMix = NSI 041816AVOC: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 71% Analysis Date = 07/29/16 SpikeMix = Phenova B20160319: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 93% Analysis Date = 06/10/16 SpikeMix = NSI 041816AVOC: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 73% Analysis Date = 09/28/16 SpikeMix = Crescent 03FF058: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 71% Analysis Date = 09/08/16 SpikeMix = Phenova B20160319: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 87% Analysis Date = 08/20/16 SpikeMix = Accu 216041125: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 76% Analysis Date = 11/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 79% Analysis Date = 10/17/15 SpikeMix = Crescent 04EE008: 15 µl & NSI 050515AVOC: 15 µl Pct Recovery = 81% Analysis Date = 06/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Accu 215041380: 15 µl Pct Recovery = 72% Analysis Date = 04/26/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 97% Analysis Date = 03/04/16 SpikeMix = Accu 215041380: 15 µl & ERA 0406-15-03: 15 µl Pct Recovery = 86% Analysis Date = 02/05/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 71% Analysis Date = 10/16/15 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 82% Analysis Date = 04/09/15 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 79% Analysis Date = 08/19/14 SpikeMix = Spex Organics C1140417015: 20 µl & Accu 214031115: 20 µl Pct Recovery = 77% Analysis Date = 07/01/14 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 89% Analysis Date = 05/01/14 SpikeMix = Accu 214031115: 20 µl & NSI 032614: 20 µl Pct Recovery = 71% Analysis Date = 03/19/15 SpikeMix = Spex Organics C1140417015: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 78% Analysis Date = 12/17/14 SpikeMix = Supelco LC06438: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 73% Analysis Date = 11/14/14 SpikeMix = Crescent 03DD004: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 81% Analysis Date = 06/10/14 SpikeMix = Crescent 03DD004: 20 µl & NSI 032614: 20 µl Pct Recovery = 72% Analysis Date = 03/17/16 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 94% Analysis Date = 01/27/16 SpikeMix = Crescent 04EE008: 10 µl & NSI 050515AVOC: 10 µl Pct Recovery = 70% Analysis Date = 12/10/15 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 80% Analysis Date = 09/03/15 SpikeMix = NSI 050515AVOC: 10 µl & Spex Organics EN150428007: 10 µl Pct Recovery = 90% Analysis Date = 11/20/15 SpikeMix = Accu 215041380: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 79% Analysis Date = 07/31/15 SpikeMix = Crescent 04EE008: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 69% Analysis Date = 06/27/15 SpikeMix = ERA 0406-15-03: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 83% Analysis Date = 09/09/14 SpikeMix = Accu 214031115: 10 µl & NSI 032614: 10 µl Pct Recovery = 94% Analysis Date = 07/23/14 SpikeMix = Spex Organics C1140417015: 10 µl & Accu 214031115: 10 µl Pct Recovery = 79% Analysis Date = 06/18/14 SpikeMix = Supelco LC06438: 10 µl & Accu 214031115: 10 µl Pct Recovery = 100% Analysis Date = 07/29/14 SpikeMix = Crescent 03DD004: 10 µl & NSI 032614: 10 µl Pct Recovery = 91% Analysis Date = 05/03/14 SpikeMix = Crescent 03DD004: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 78% Analysis Date = 01/13/15 SpikeMix = Accu 214031115: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 75% Analysis Date = 11/06/14 SpikeMix = Spex Organics C1140417015: 10 µl & Crescent 03DD004: 10 µl Pct Recovery = 80% Analysis Date = 10/04/14 SpikeMix = Crescent 03DD004: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 90% Analysis Date = 12/15/16 Pct Recovery = 83% Analysis Date = 12/11/16 Pct Recovery = 83% Analysis Date = 12/11/16 Pct Recovery = 83% Analysis Date = 12/06/16 Pct Recovery = 83% Analysis Date = 12/06/16 Pct Recovery = 83% Analysis Date = 12/01/16 Pct Recovery = 83% Analysis Date = 12/01/16 Pct Recovery = 83% Analysis Date = 11/26/16 Pct Recovery = 83% Analysis Date = 11/26/16 Pct Recovery = 83% Analysis Date = 11/21/16 Pct Recovery = 83% Analysis Date = 11/21/16 Pct Recovery = 83% Analysis Date = 11/17/16 Pct Recovery = 83% Analysis Date = 11/17/16 Pct Recovery = 83% Analysis Date = 11/12/16 Pct Recovery = 83% Analysis Date = 11/12/16 Pct Recovery = 83% Analysis Date = 11/07/16 Pct Recovery = 83% Analysis Date = 11/07/16 Pct Recovery = 83% Analysis Date = 11/02/16 Pct Recovery = 83% Analysis Date = 11/02/16 Pct Recovery = 83% Analysis Date = 10/28/16 Pct Recovery = 83% Analysis Date = 10/28/16 Pct Recovery = 83% Analysis Date = 10/24/16 Pct Recovery = 83% Analysis Date = 10/24/16 Pct Recovery = 83% Analysis Date = 10/19/16 Pct Recovery = 83% Analysis Date = 10/19/16 Pct Recovery = 83% Analysis Date = 10/14/16 Pct Recovery = 83% Analysis Date = 10/14/16 Pct Recovery = 83% Analysis Date = 10/09/16 Pct Recovery = 83% Analysis Date = 10/09/16 Pct Recovery = 83% Analysis Date = 10/04/16 Pct Recovery = 83% Analysis Date = 10/04/16 Pct Recovery = 83% Analysis Date = 09/30/16 Pct Recovery = 83% Analysis Date = 09/30/16 Pct Recovery = 83% Analysis Date = 09/25/16 Pct Recovery = 83% Analysis Date = 09/25/16 Pct Recovery = 83% Analysis Date = 09/20/16 Pct Recovery = 83% Analysis Date = 09/20/16 Pct Recovery = 83% Analysis Date = 09/15/16 Pct Recovery = 83% Analysis Date = 09/15/16 Pct Recovery = 83% Analysis Date = 09/10/16 Pct Recovery = 83% Analysis Date = 09/10/16 Pct Recovery = 83% Analysis Date = 09/06/16 Pct Recovery = 83% Analysis Date = 09/06/16 Pct Recovery = 83% Analysis Date = 09/01/16 Pct Recovery = 83% Analysis Date = 09/01/16 Pct Recovery = 83% Analysis Date = 08/27/16 Pct Recovery = 83% Analysis Date = 08/27/16 Pct Recovery = 83% Analysis Date = 08/22/16 Pct Recovery = 83% Analysis Date = 08/22/16 Pct Recovery = 83% Analysis Date = 08/17/16 Pct Recovery = 83% Analysis Date = 08/17/16 Pct Recovery = 83% Analysis Date = 08/13/16 Pct Recovery = 83% Analysis Date = 08/13/16 Pct Recovery = 83% Analysis Date = 08/08/16 Pct Recovery = 83% Analysis Date = 08/08/16 Pct Recovery = 83% Analysis Date = 08/03/16 Pct Recovery = 83% Analysis Date = 08/03/16 Pct Recovery = 83% Analysis Date = 07/29/16 Pct Recovery = 83% Analysis Date = 07/29/16 Pct Recovery = 83% Analysis Date = 07/24/16 Pct Recovery = 83% Analysis Date = 07/24/16 Pct Recovery = 83% Analysis Date = 07/20/16 Pct Recovery = 83% Analysis Date = 07/20/16 Pct Recovery = 83% Analysis Date = 07/15/16 Pct Recovery = 83% Analysis Date = 07/15/16 Pct Recovery = 83% Analysis Date = 07/10/16 Pct Recovery = 83% Analysis Date = 07/10/16 Pct Recovery = 83% Analysis Date = 07/05/16 Pct Recovery = 83% Analysis Date = 07/05/16 Pct Recovery = 83% Analysis Date = 06/30/16 Pct Recovery = 83% Analysis Date = 06/30/16 Pct Recovery = 83% Analysis Date = 06/26/16 Pct Recovery = 83% Analysis Date = 06/26/16 Pct Recovery = 83% Analysis Date = 06/21/16 Pct Recovery = 83% Analysis Date = 06/21/16 Pct Recovery = 83% Analysis Date = 06/16/16 Pct Recovery = 83% Analysis Date = 06/16/16 Pct Recovery = 83% Analysis Date = 06/11/16 Pct Recovery = 83% Analysis Date = 06/11/16 Pct Recovery = 83% Analysis Date = 06/06/16 Pct Recovery = 83% Analysis Date = 06/06/16 Pct Recovery = 83% Analysis Date = 06/02/16 Pct Recovery = 83% Analysis Date = 06/02/16 Pct Recovery = 83% Analysis Date = 05/28/16 Pct Recovery = 83% Analysis Date = 05/28/16 Pct Recovery = 83% Analysis Date = 05/23/16 Pct Recovery = 83% Analysis Date = 05/23/16 Pct Recovery = 83% Analysis Date = 05/18/16 Pct Recovery = 83% Analysis Date = 05/18/16 Pct Recovery = 83% Analysis Date = 05/13/16 Pct Recovery = 83% Analysis Date = 05/13/16 Pct Recovery = 83% Analysis Date = 05/09/16 Pct Recovery = 83% Analysis Date = 05/09/16 Pct Recovery = 83% Analysis Date = 05/04/16 Pct Recovery = 83% Analysis Date = 05/04/16 Pct Recovery = 83% Analysis Date = 04/29/16 Pct Recovery = 82% Analysis Date = 04/29/16 Pct Recovery = 82% Analysis Date = 04/24/16 Pct Recovery = 82% Analysis Date = 04/24/16 Pct Recovery = 82% Analysis Date = 04/19/16 Pct Recovery = 82% Analysis Date = 04/19/16 Pct Recovery = 82% Analysis Date = 04/15/16 Pct Recovery = 82% Analysis Date = 04/15/16 Pct Recovery = 82% Analysis Date = 04/10/16 Pct Recovery = 82% Analysis Date = 04/10/16 Pct Recovery = 82% Analysis Date = 04/05/16 Pct Recovery = 82% Analysis Date = 04/05/16 Pct Recovery = 82% Analysis Date = 03/31/16 Pct Recovery = 82% Analysis Date = 03/31/16 Pct Recovery = 82% Analysis Date = 03/26/16 Pct Recovery = 82% Analysis Date = 03/26/16 Pct Recovery = 82% Analysis Date = 03/22/16 Pct Recovery = 82% Analysis Date = 03/22/16 Pct Recovery = 82% Analysis Date = 03/17/16 Pct Recovery = 82% Analysis Date = 03/17/16 Pct Recovery = 82% Analysis Date = 03/12/16 Pct Recovery = 82% Analysis Date = 03/12/16 Pct Recovery = 82% Analysis Date = 03/07/16 Pct Recovery = 82% Analysis Date = 03/07/16 Pct Recovery = 82% Analysis Date = 03/02/16 Pct Recovery = 82% Analysis Date = 03/02/16 Pct Recovery = 82% Analysis Date = 02/27/16 Pct Recovery = 82% Analysis Date = 02/27/16 Pct Recovery = 82% Analysis Date = 02/22/16 Pct Recovery = 82% Analysis Date = 02/22/16 Pct Recovery = 82% Analysis Date = 02/17/16 Pct Recovery = 82% Analysis Date = 02/17/16 Pct Recovery = 82% Analysis Date = 02/12/16 Pct Recovery = 82% Analysis Date = 02/12/16 Pct Recovery = 82% Analysis Date = 02/07/16 Pct Recovery = 82% Analysis Date = 02/07/16 Pct Recovery = 82% Analysis Date = 02/03/16 Pct Recovery = 82% Analysis Date = 02/03/16 Pct Recovery = 82% Analysis Date = 01/29/16 Pct Recovery = 82% Analysis Date = 01/29/16 Pct Recovery = 82% Analysis Date = 01/24/16 Pct Recovery = 81% Analysis Date = 01/24/16 Pct Recovery = 81% Analysis Date = 01/19/16 Pct Recovery = 81% Analysis Date = 01/19/16 Pct Recovery = 81% Analysis Date = 01/14/16 Pct Recovery = 81% Analysis Date = 01/14/16 Pct Recovery = 81% Analysis Date = 01/10/16 Pct Recovery = 81% Analysis Date = 01/10/16 Pct Recovery = 81% Analysis Date = 01/05/16 Pct Recovery = 81% Analysis Date = 01/05/16 Pct Recovery = 81% Analysis Date = 12/31/15 Pct Recovery = 81% Analysis Date = 12/31/15 Pct Recovery = 81% Analysis Date = 12/26/15 Pct Recovery = 81% Analysis Date = 12/26/15 Pct Recovery = 81% Analysis Date = 12/21/15 Pct Recovery = 81% Analysis Date = 12/21/15 Pct Recovery = 81% Analysis Date = 12/17/15 Pct Recovery = 81% Analysis Date = 12/17/15 Pct Recovery = 81% Analysis Date = 12/12/15 Pct Recovery = 81% Analysis Date = 12/12/15 Pct Recovery = 81% Analysis Date = 12/07/15 Pct Recovery = 80% Analysis Date = 12/07/15 Pct Recovery = 80% Analysis Date = 12/02/15 Pct Recovery = 80% Analysis Date = 12/02/15 Pct Recovery = 80% Analysis Date = 11/27/15 Pct Recovery = 80% Analysis Date = 11/27/15 Pct Recovery = 80% Analysis Date = 11/23/15 Pct Recovery = 80% Analysis Date = 11/23/15 Pct Recovery = 80% Analysis Date = 11/18/15 Pct Recovery = 80% Analysis Date = 11/18/15 Pct Recovery = 80% Analysis Date = 11/13/15 Pct Recovery = 80% Analysis Date = 11/13/15 Pct Recovery = 80% Analysis Date = 11/08/15 Pct Recovery = 80% Analysis Date = 11/08/15 Pct Recovery = 80% Analysis Date = 11/03/15 Pct Recovery = 80% Analysis Date = 11/03/15 Pct Recovery = 80% Analysis Date = 10/30/15 Pct Recovery = 79% Analysis Date = 10/30/15 Pct Recovery = 79% Analysis Date = 10/25/15 Pct Recovery = 79% Analysis Date = 10/25/15 Pct Recovery = 79% Analysis Date = 10/20/15 Pct Recovery = 79% Analysis Date = 10/20/15 Pct Recovery = 79% Analysis Date = 10/15/15 Pct Recovery = 79% Analysis Date = 10/15/15 Pct Recovery = 79% Analysis Date = 10/10/15 Pct Recovery = 79% Analysis Date = 10/10/15 Pct Recovery = 79% Analysis Date = 10/06/15 Pct Recovery = 79% Analysis Date = 10/06/15 Pct Recovery = 79% Analysis Date = 10/01/15 Pct Recovery = 79% Analysis Date = 10/01/15 Pct Recovery = 79% Analysis Date = 09/26/15 Pct Recovery = 79% Analysis Date = 09/26/15 Pct Recovery = 79% Analysis Date = 09/21/15 Pct Recovery = 79% Analysis Date = 09/21/15 Pct Recovery = 79% Analysis Date = 09/16/15 Pct Recovery = 78% Analysis Date = 09/16/15 Pct Recovery = 78% Analysis Date = 09/12/15 Pct Recovery = 78% Analysis Date = 09/12/15 Pct Recovery = 78% Analysis Date = 09/07/15 Pct Recovery = 78% Analysis Date = 09/07/15 Pct Recovery = 78% Analysis Date = 09/02/15 Pct Recovery = 78% Analysis Date = 09/02/15 Pct Recovery = 78% Analysis Date = 08/28/15 Pct Recovery = 78% Analysis Date = 08/28/15 Pct Recovery = 78% Analysis Date = 08/23/15 Pct Recovery = 78% Analysis Date = 08/23/15 Pct Recovery = 78% Analysis Date = 08/19/15 Pct Recovery = 78% Analysis Date = 08/19/15 Pct Recovery = 78% Analysis Date = 08/14/15 Pct Recovery = 78% Analysis Date = 08/14/15 Pct Recovery = 78% Analysis Date = 08/09/15 Pct Recovery = 78% Analysis Date = 08/09/15 Pct Recovery = 78% Analysis Date = 08/04/15 Pct Recovery = 78% Analysis Date = 08/04/15 Pct Recovery = 78% Analysis Date = 07/30/15 Pct Recovery = 78% Analysis Date = 07/30/15 Pct Recovery = 78% Analysis Date = 07/26/15 Pct Recovery = 78% Analysis Date = 07/26/15 Pct Recovery = 78% Analysis Date = 07/21/15 Pct Recovery = 78% Analysis Date = 07/21/15 Pct Recovery = 78% Analysis Date = 07/16/15 Pct Recovery = 78% Analysis Date = 07/16/15 Pct Recovery = 78% Analysis Date = 07/11/15 Pct Recovery = 78% Analysis Date = 07/11/15 Pct Recovery = 78% Analysis Date = 07/06/15 Pct Recovery = 78% Analysis Date = 07/06/15 Pct Recovery = 78% Analysis Date = 07/02/15 Pct Recovery = 78% Analysis Date = 07/02/15 Pct Recovery = 78% Analysis Date = 06/27/15 Pct Recovery = 78% Analysis Date = 06/27/15 Pct Recovery = 78% Analysis Date = 06/22/15 Pct Recovery = 78% Analysis Date = 06/22/15 Pct Recovery = 78% Analysis Date = 06/17/15 Pct Recovery = 78% Analysis Date = 06/17/15 Pct Recovery = 78% Analysis Date = 06/12/15 Pct Recovery = 78% Analysis Date = 06/12/15 Pct Recovery = 78% Analysis Date = 06/08/15 Pct Recovery = 78% Analysis Date = 06/08/15 Pct Recovery = 78% Analysis Date = 06/03/15 Pct Recovery = 78% Analysis Date = 06/03/15 Pct Recovery = 78% Analysis Date = 05/29/15 Pct Recovery = 78% Analysis Date = 05/29/15 Pct Recovery = 78% Analysis Date = 05/24/15 Pct Recovery = 78% Analysis Date = 05/24/15 Pct Recovery = 78% Analysis Date = 05/19/15 Pct Recovery = 78% Analysis Date = 05/19/15 Pct Recovery = 78% Analysis Date = 05/15/15 Pct Recovery = 78% Analysis Date = 05/15/15 Pct Recovery = 78% Analysis Date = 05/10/15 Pct Recovery = 78% Analysis Date = 05/10/15 Pct Recovery = 78% Analysis Date = 05/05/15 Pct Recovery = 78% Analysis Date = 05/05/15 Pct Recovery = 78% Analysis Date = 04/30/15 Pct Recovery = 78% Analysis Date = 04/30/15 Pct Recovery = 78% Analysis Date = 04/25/15 Pct Recovery = 78% Analysis Date = 04/25/15 Pct Recovery = 78% Analysis Date = 04/21/15 Pct Recovery = 78% Analysis Date = 04/21/15 Pct Recovery = 78% Analysis Date = 04/16/15 Pct Recovery = 78% Analysis Date = 04/16/15 Pct Recovery = 78% Analysis Date = 04/11/15 Pct Recovery = 79% Analysis Date = 04/11/15 Pct Recovery = 79% Analysis Date = 04/06/15 Pct Recovery = 79% Analysis Date = 04/06/15 Pct Recovery = 79% Analysis Date = 04/01/15 Pct Recovery = 79% Analysis Date = 04/01/15 Pct Recovery = 79% Analysis Date = 03/28/15 Pct Recovery = 79% Analysis Date = 03/28/15 Pct Recovery = 79% Analysis Date = 03/23/15 Pct Recovery = 79% Analysis Date = 03/23/15 Pct Recovery = 79% Analysis Date = 03/18/15 Pct Recovery = 79% Analysis Date = 03/18/15 Pct Recovery = 79% Analysis Date = 03/13/15 Pct Recovery = 79% Analysis Date = 03/13/15 Pct Recovery = 79% Analysis Date = 03/08/15 Pct Recovery = 79% Analysis Date = 03/08/15 Pct Recovery = 79% Analysis Date = 03/04/15 Pct Recovery = 79% Analysis Date = 03/04/15 Pct Recovery = 79% Analysis Date = 02/27/15 Pct Recovery = 79% Analysis Date = 02/27/15 Pct Recovery = 79% Analysis Date = 02/22/15 Pct Recovery = 79% Analysis Date = 02/22/15 Pct Recovery = 79% Analysis Date = 02/17/15 Pct Recovery = 79% Analysis Date = 02/17/15 Pct Recovery = 79% Analysis Date = 02/12/15 Pct Recovery = 79% Analysis Date = 02/12/15 Pct Recovery = 79% Analysis Date = 02/08/15 Pct Recovery = 80% Analysis Date = 02/08/15 Pct Recovery = 80% Analysis Date = 02/03/15 Pct Recovery = 80% Analysis Date = 02/03/15 Pct Recovery = 80% Analysis Date = 01/29/15 Pct Recovery = 80% Analysis Date = 01/29/15 Pct Recovery = 80% Analysis Date = 01/24/15 Pct Recovery = 80% Analysis Date = 01/24/15 Pct Recovery = 80% Analysis Date = 01/19/15 Pct Recovery = 80% Analysis Date = 01/19/15 Pct Recovery = 80% Analysis Date = 01/15/15 Pct Recovery = 80% Analysis Date = 01/15/15 Pct Recovery = 80% Analysis Date = 01/10/15 Pct Recovery = 80% Analysis Date = 01/10/15 Pct Recovery = 80% Analysis Date = 01/05/15 Pct Recovery = 80% Analysis Date = 01/05/15 Pct Recovery = 80% Analysis Date = 12/31/14 Pct Recovery = 80% Analysis Date = 12/31/14 Pct Recovery = 80% Analysis Date = 12/26/14 Pct Recovery = 80% Analysis Date = 12/26/14 Pct Recovery = 80% Analysis Date = 12/22/14 Pct Recovery = 80% Analysis Date = 12/22/14 Pct Recovery = 80% Analysis Date = 12/17/14 Pct Recovery = 80% Analysis Date = 12/17/14 Pct Recovery = 80% Analysis Date = 12/12/14 Pct Recovery = 80% Analysis Date = 12/12/14 Pct Recovery = 80% Analysis Date = 12/07/14 Pct Recovery = 80% Analysis Date = 12/07/14 Pct Recovery = 80% Analysis Date = 12/02/14 Pct Recovery = 81% Analysis Date = 12/02/14 Pct Recovery = 81% Analysis Date = 11/28/14 Pct Recovery = 81% Analysis Date = 11/28/14 Pct Recovery = 81% Analysis Date = 11/23/14 Pct Recovery = 81% Analysis Date = 11/23/14 Pct Recovery = 81% Analysis Date = 11/18/14 Pct Recovery = 81% Analysis Date = 11/18/14 Pct Recovery = 81% Analysis Date = 11/13/14 Pct Recovery = 81% Analysis Date = 11/13/14 Pct Recovery = 81% Analysis Date = 11/08/14 Pct Recovery = 81% Analysis Date = 11/08/14 Pct Recovery = 81% Analysis Date = 11/04/14 Pct Recovery = 81% Analysis Date = 11/04/14 Pct Recovery = 81% Analysis Date = 10/30/14 Pct Recovery = 81% Analysis Date = 10/30/14 Pct Recovery = 81% Analysis Date = 10/25/14 Pct Recovery = 81% Analysis Date = 10/25/14 Pct Recovery = 81% Analysis Date = 10/20/14 Pct Recovery = 81% Analysis Date = 10/20/14 Pct Recovery = 81% Analysis Date = 10/15/14 Pct Recovery = 81% Analysis Date = 10/15/14 Pct Recovery = 81% Analysis Date = 10/11/14 Pct Recovery = 81% Analysis Date = 10/11/14 Pct Recovery = 81% Analysis Date = 10/06/14 Pct Recovery = 81% Analysis Date = 10/06/14 Pct Recovery = 81% Analysis Date = 10/01/14 Pct Recovery = 81% Analysis Date = 10/01/14 Pct Recovery = 81% Analysis Date = 09/26/14 Pct Recovery = 81% Analysis Date = 09/26/14 Pct Recovery = 81% Analysis Date = 09/21/14 Pct Recovery = 81% Analysis Date = 09/21/14 Pct Recovery = 81% Analysis Date = 09/17/14 Pct Recovery = 82% Analysis Date = 09/17/14 Pct Recovery = 82% Analysis Date = 09/12/14 Pct Recovery = 82% Analysis Date = 09/12/14 Pct Recovery = 82% Analysis Date = 09/07/14 Pct Recovery = 82% Analysis Date = 09/07/14 Pct Recovery = 82% Analysis Date = 09/02/14 Pct Recovery = 82% Analysis Date = 09/02/14 Pct Recovery = 82% Analysis Date = 08/28/14 Pct Recovery = 82% Analysis Date = 08/28/14 Pct Recovery = 82% Analysis Date = 08/24/14 Pct Recovery = 82% Analysis Date = 08/24/14 Pct Recovery = 82% Analysis Date = 08/19/14 Pct Recovery = 82% Analysis Date = 08/19/14 Pct Recovery = 82% Analysis Date = 08/14/14 Pct Recovery = 82% Analysis Date = 08/14/14 Pct Recovery = 82% Analysis Date = 08/09/14 Pct Recovery = 82% Analysis Date = 08/09/14 Pct Recovery = 82% Analysis Date = 08/04/14 Pct Recovery = 82% Analysis Date = 08/04/14 Pct Recovery = 82% Analysis Date = 07/31/14 Pct Recovery = 82% Analysis Date = 07/31/14 Pct Recovery = 82% Analysis Date = 07/26/14 Pct Recovery = 82% Analysis Date = 07/26/14 Pct Recovery = 82% Analysis Date = 07/21/14 Pct Recovery = 82% Analysis Date = 07/21/14 Pct Recovery = 82% Analysis Date = 07/16/14 Pct Recovery = 82% Analysis Date = 07/16/14 Pct Recovery = 82% Analysis Date = 07/11/14 Pct Recovery = 83% Analysis Date = 07/11/14 Pct Recovery = 83% Analysis Date = 07/07/14 Pct Recovery = 83% Analysis Date = 07/07/14 Pct Recovery = 83% Analysis Date = 07/02/14 Pct Recovery = 83% Analysis Date = 07/02/14 Pct Recovery = 83% Analysis Date = 06/27/14 Pct Recovery = 83% Analysis Date = 06/27/14 Pct Recovery = 83% Analysis Date = 06/22/14 Pct Recovery = 83% Analysis Date = 06/22/14 Pct Recovery = 83% Analysis Date = 06/17/14 Pct Recovery = 83% Analysis Date = 06/17/14 Pct Recovery = 83% Analysis Date = 06/13/14 Pct Recovery = 83% Analysis Date = 06/13/14 Pct Recovery = 83% Analysis Date = 06/08/14 Pct Recovery = 83% Analysis Date = 06/08/14 Pct Recovery = 83% Analysis Date = 06/03/14 Pct Recovery = 83% Analysis Date = 06/03/14 Pct Recovery = 83% Analysis Date = 05/29/14 Pct Recovery = 83% Analysis Date = 05/29/14 Pct Recovery = 83% Analysis Date = 05/24/14 Pct Recovery = 83% Analysis Date = 05/24/14 Pct Recovery = 83% Analysis Date = 05/20/14 Pct Recovery = 83% Analysis Date = 05/20/14 Pct Recovery = 83% Analysis Date = 05/15/14 Pct Recovery = 83% Analysis Date = 05/15/14 Pct Recovery = 83% Analysis Date = 05/10/14 Pct Recovery = 84% Analysis Date = 05/10/14 Pct Recovery = 84% Analysis Date = 05/05/14 Pct Recovery = 84% Analysis Date = 05/05/14 Pct Recovery = 84% Analysis Date = 05/01/14 Pct Recovery = 84% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
1,2-DIBROMO-3-CHLOROPROPANE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 3 81% 8% 80% 11%
>= Reporting Level 46 81% 8% 80% 10%
Total 49 81% 8% 80% 9%

Sample Statistics
1,2-DIBROMO-3-CHLOROPROPANE

Characteristic N % % Basis
Plotted 49 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 49 .  
False Negatives 0 0% 0 out of 49
Not Spiked 24 .  
False Positives 0 0% 0 out of 24

BQS OBSP Determination:
1,2-DIBROMOETHANE
METHOD: 4440 , TESTIDCODE: 77651GCM66
Open Data Set

Analysis Date = 12/12/16 SpikeMix = Accu 216041125: 40 µl & Crescent 03FF058: 40 µl Pct Recovery = 103% Analysis Date = 07/20/16 SpikeMix = Supelco LC20141V: 40 µl & Accu 216041125: 40 µl Pct Recovery = 94% Analysis Date = 07/14/16 SpikeMix = Accu 216041125: 40 µl & NSI 041816AVOC: 40 µl Pct Recovery = 94% Analysis Date = 08/12/16 SpikeMix = ChemService 5082900: 25 µl & Phenova B20160319: 25 µl Pct Recovery = 91% Analysis Date = 06/21/16 SpikeMix = Phenova B20160319: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 105% Analysis Date = 09/08/16 SpikeMix = Supelco LC20141V: 25 µl & Accu 216041125: 25 µl Pct Recovery = 85% Analysis Date = 05/24/16 SpikeMix = Accu 216041125: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 94% Analysis Date = 04/09/15 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 104% Analysis Date = 03/06/15 SpikeMix = ERA 0227-14-06.1A: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 103% Analysis Date = 11/14/14 SpikeMix = Crescent 03DD004: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 95% Analysis Date = 08/16/14 SpikeMix = ERA 0227-14-06.1A: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 98% Analysis Date = 07/01/14 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 102% Analysis Date = 11/22/14 SpikeMix = NSI 032614: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 93% Analysis Date = 06/10/14 SpikeMix = Crescent 03DD004: 20 µl & NSI 032614: 20 µl Pct Recovery = 88% Analysis Date = 06/10/14 SpikeMix = NSI 032614: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 99% Analysis Date = 05/01/14 SpikeMix = Accu 214031115: 20 µl & NSI 032614: 20 µl Pct Recovery = 89% Analysis Date = 07/13/15 SpikeMix = Crescent 04EE008: 25 µl & NSI 050515AVOC: 25 µl Pct Recovery = 122% Analysis Date = 09/29/15 SpikeMix = Accu 215041380: 25 µl & ERA 0406-15-03: 25 µl Pct Recovery = 100% Analysis Date = 06/16/15 SpikeMix = ERA 0406-15-03: 25 µl & Supelco LC13545: 25 µl Pct Recovery = 87% Analysis Date = 11/29/16 SpikeMix = ChemService 5082900: 15 µl & Phenova B20160319: 15 µl Pct Recovery = 100% Analysis Date = 09/08/16 SpikeMix = Phenova B20160319: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 100% Analysis Date = 07/29/16 SpikeMix = Phenova B20160319: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 100% Analysis Date = 05/27/16 SpikeMix = Phenova B20160319: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 96% Analysis Date = 10/13/16 SpikeMix = Accu 216041125: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 107% Analysis Date = 08/20/16 SpikeMix = Accu 216041125: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 106% Analysis Date = 06/30/16 SpikeMix = ChemService 5082900: 15 µl & Accu 216041125: 15 µl Pct Recovery = 74% Analysis Date = 11/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 129% Analysis Date = 10/17/15 SpikeMix = Crescent 04EE008: 15 µl & NSI 050515AVOC: 15 µl Pct Recovery = 118% Analysis Date = 06/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Accu 215041380: 15 µl Pct Recovery = 125% Analysis Date = 04/26/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 118% Analysis Date = 03/04/16 SpikeMix = Accu 215041380: 15 µl & ERA 0406-15-03: 15 µl Pct Recovery = 88% Analysis Date = 02/05/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 94% Analysis Date = 10/16/15 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 111% Analysis Date = 01/13/15 SpikeMix = Accu 214031115: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 97% Analysis Date = 10/21/14 SpikeMix = ERA 0227-14-06.1A: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 88% Analysis Date = 10/04/14 SpikeMix = Crescent 03DD004: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 102% Analysis Date = 07/11/14 SpikeMix = Spex Organics C1140417015: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 95% Analysis Date = 09/09/14 SpikeMix = Accu 214031115: 10 µl & NSI 032614: 10 µl Pct Recovery = 126% Analysis Date = 09/09/14 SpikeMix = NSI 032614: 10 µl & Spex Organics C1140417015: 10 µl Pct Recovery = 116% Analysis Date = 07/29/14 SpikeMix = Crescent 03DD004: 10 µl & NSI 032614: 10 µl Pct Recovery = 108% Analysis Date = 05/30/14 SpikeMix = NSI 032614: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 82% Analysis Date = 03/17/16 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 114% Analysis Date = 01/27/16 SpikeMix = Crescent 04EE008: 10 µl & NSI 050515AVOC: 10 µl Pct Recovery = 124% Analysis Date = 12/10/15 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 125% Analysis Date = 09/03/15 SpikeMix = NSI 050515AVOC: 10 µl & Spex Organics EN150428007: 10 µl Pct Recovery = 132% Analysis Date = 11/20/15 SpikeMix = Accu 215041380: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 96% Analysis Date = 07/31/15 SpikeMix = Crescent 04EE008: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 83% Analysis Date = 06/27/15 SpikeMix = ERA 0406-15-03: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 102% Analysis Date = 12/11/16 Pct Recovery = 95% Analysis Date = 12/07/16 Pct Recovery = 95% Analysis Date = 12/07/16 Pct Recovery = 95% Analysis Date = 12/02/16 Pct Recovery = 95% Analysis Date = 12/02/16 Pct Recovery = 95% Analysis Date = 11/27/16 Pct Recovery = 95% Analysis Date = 11/27/16 Pct Recovery = 95% Analysis Date = 11/22/16 Pct Recovery = 95% Analysis Date = 11/22/16 Pct Recovery = 95% Analysis Date = 11/18/16 Pct Recovery = 95% Analysis Date = 11/18/16 Pct Recovery = 95% Analysis Date = 11/13/16 Pct Recovery = 95% Analysis Date = 11/13/16 Pct Recovery = 95% Analysis Date = 11/08/16 Pct Recovery = 96% Analysis Date = 11/08/16 Pct Recovery = 96% Analysis Date = 11/03/16 Pct Recovery = 96% Analysis Date = 11/03/16 Pct Recovery = 96% Analysis Date = 10/29/16 Pct Recovery = 96% Analysis Date = 10/29/16 Pct Recovery = 96% Analysis Date = 10/25/16 Pct Recovery = 96% Analysis Date = 10/25/16 Pct Recovery = 96% Analysis Date = 10/20/16 Pct Recovery = 96% Analysis Date = 10/20/16 Pct Recovery = 96% Analysis Date = 10/15/16 Pct Recovery = 96% Analysis Date = 10/15/16 Pct Recovery = 96% Analysis Date = 10/10/16 Pct Recovery = 96% Analysis Date = 10/10/16 Pct Recovery = 96% Analysis Date = 10/06/16 Pct Recovery = 96% Analysis Date = 10/06/16 Pct Recovery = 96% Analysis Date = 10/01/16 Pct Recovery = 97% Analysis Date = 10/01/16 Pct Recovery = 97% Analysis Date = 09/26/16 Pct Recovery = 97% Analysis Date = 09/26/16 Pct Recovery = 97% Analysis Date = 09/21/16 Pct Recovery = 97% Analysis Date = 09/21/16 Pct Recovery = 97% Analysis Date = 09/16/16 Pct Recovery = 97% Analysis Date = 09/16/16 Pct Recovery = 97% Analysis Date = 09/12/16 Pct Recovery = 97% Analysis Date = 09/12/16 Pct Recovery = 97% Analysis Date = 09/07/16 Pct Recovery = 97% Analysis Date = 09/07/16 Pct Recovery = 97% Analysis Date = 09/02/16 Pct Recovery = 97% Analysis Date = 09/02/16 Pct Recovery = 97% Analysis Date = 08/28/16 Pct Recovery = 98% Analysis Date = 08/28/16 Pct Recovery = 98% Analysis Date = 08/24/16 Pct Recovery = 98% Analysis Date = 08/24/16 Pct Recovery = 98% Analysis Date = 08/19/16 Pct Recovery = 98% Analysis Date = 08/19/16 Pct Recovery = 98% Analysis Date = 08/14/16 Pct Recovery = 98% Analysis Date = 08/14/16 Pct Recovery = 98% Analysis Date = 08/09/16 Pct Recovery = 98% Analysis Date = 08/09/16 Pct Recovery = 98% Analysis Date = 08/04/16 Pct Recovery = 98% Analysis Date = 08/04/16 Pct Recovery = 98% Analysis Date = 07/31/16 Pct Recovery = 99% Analysis Date = 07/31/16 Pct Recovery = 99% Analysis Date = 07/26/16 Pct Recovery = 99% Analysis Date = 07/26/16 Pct Recovery = 99% Analysis Date = 07/21/16 Pct Recovery = 99% Analysis Date = 07/21/16 Pct Recovery = 99% Analysis Date = 07/16/16 Pct Recovery = 99% Analysis Date = 07/16/16 Pct Recovery = 99% Analysis Date = 07/12/16 Pct Recovery = 99% Analysis Date = 07/12/16 Pct Recovery = 99% Analysis Date = 07/07/16 Pct Recovery = 99% Analysis Date = 07/07/16 Pct Recovery = 99% Analysis Date = 07/02/16 Pct Recovery = 100% Analysis Date = 07/02/16 Pct Recovery = 100% Analysis Date = 06/27/16 Pct Recovery = 100% Analysis Date = 06/27/16 Pct Recovery = 100% Analysis Date = 06/22/16 Pct Recovery = 100% Analysis Date = 06/22/16 Pct Recovery = 100% Analysis Date = 06/18/16 Pct Recovery = 100% Analysis Date = 06/18/16 Pct Recovery = 100% Analysis Date = 06/13/16 Pct Recovery = 100% Analysis Date = 06/13/16 Pct Recovery = 100% Analysis Date = 06/08/16 Pct Recovery = 100% Analysis Date = 06/08/16 Pct Recovery = 100% Analysis Date = 06/03/16 Pct Recovery = 101% Analysis Date = 06/03/16 Pct Recovery = 101% Analysis Date = 05/30/16 Pct Recovery = 101% Analysis Date = 05/30/16 Pct Recovery = 101% Analysis Date = 05/25/16 Pct Recovery = 101% Analysis Date = 05/25/16 Pct Recovery = 101% Analysis Date = 05/20/16 Pct Recovery = 101% Analysis Date = 05/20/16 Pct Recovery = 101% Analysis Date = 05/15/16 Pct Recovery = 101% Analysis Date = 05/15/16 Pct Recovery = 101% Analysis Date = 05/10/16 Pct Recovery = 102% Analysis Date = 05/10/16 Pct Recovery = 102% Analysis Date = 05/06/16 Pct Recovery = 102% Analysis Date = 05/06/16 Pct Recovery = 102% Analysis Date = 05/01/16 Pct Recovery = 102% Analysis Date = 05/01/16 Pct Recovery = 102% Analysis Date = 04/26/16 Pct Recovery = 102% Analysis Date = 04/26/16 Pct Recovery = 102% Analysis Date = 04/21/16 Pct Recovery = 103% Analysis Date = 04/21/16 Pct Recovery = 103% Analysis Date = 04/16/16 Pct Recovery = 103% Analysis Date = 04/16/16 Pct Recovery = 103% Analysis Date = 04/12/16 Pct Recovery = 103% Analysis Date = 04/12/16 Pct Recovery = 103% Analysis Date = 04/07/16 Pct Recovery = 103% Analysis Date = 04/07/16 Pct Recovery = 103% Analysis Date = 04/02/16 Pct Recovery = 104% Analysis Date = 04/02/16 Pct Recovery = 104% Analysis Date = 03/28/16 Pct Recovery = 104% Analysis Date = 03/28/16 Pct Recovery = 104% Analysis Date = 03/24/16 Pct Recovery = 104% Analysis Date = 03/24/16 Pct Recovery = 104% Analysis Date = 03/19/16 Pct Recovery = 104% Analysis Date = 03/19/16 Pct Recovery = 104% Analysis Date = 03/14/16 Pct Recovery = 105% Analysis Date = 03/14/16 Pct Recovery = 105% Analysis Date = 03/09/16 Pct Recovery = 105% Analysis Date = 03/09/16 Pct Recovery = 105% Analysis Date = 03/04/16 Pct Recovery = 105% Analysis Date = 03/04/16 Pct Recovery = 105% Analysis Date = 02/29/16 Pct Recovery = 105% Analysis Date = 02/29/16 Pct Recovery = 105% Analysis Date = 02/24/16 Pct Recovery = 106% Analysis Date = 02/24/16 Pct Recovery = 106% Analysis Date = 02/19/16 Pct Recovery = 106% Analysis Date = 02/19/16 Pct Recovery = 106% Analysis Date = 02/14/16 Pct Recovery = 106% Analysis Date = 02/14/16 Pct Recovery = 106% Analysis Date = 02/10/16 Pct Recovery = 107% Analysis Date = 02/10/16 Pct Recovery = 107% Analysis Date = 02/05/16 Pct Recovery = 107% Analysis Date = 02/05/16 Pct Recovery = 107% Analysis Date = 01/31/16 Pct Recovery = 107% Analysis Date = 01/31/16 Pct Recovery = 107% Analysis Date = 01/26/16 Pct Recovery = 108% Analysis Date = 01/26/16 Pct Recovery = 108% Analysis Date = 01/21/16 Pct Recovery = 108% Analysis Date = 01/21/16 Pct Recovery = 108% Analysis Date = 01/17/16 Pct Recovery = 108% Analysis Date = 01/17/16 Pct Recovery = 108% Analysis Date = 01/12/16 Pct Recovery = 108% Analysis Date = 01/12/16 Pct Recovery = 108% Analysis Date = 01/07/16 Pct Recovery = 108% Analysis Date = 01/07/16 Pct Recovery = 108% Analysis Date = 01/02/16 Pct Recovery = 108% Analysis Date = 01/02/16 Pct Recovery = 108% Analysis Date = 12/29/15 Pct Recovery = 108% Analysis Date = 12/29/15 Pct Recovery = 108% Analysis Date = 12/24/15 Pct Recovery = 108% Analysis Date = 12/24/15 Pct Recovery = 108% Analysis Date = 12/19/15 Pct Recovery = 108% Analysis Date = 12/19/15 Pct Recovery = 108% Analysis Date = 12/14/15 Pct Recovery = 108% Analysis Date = 12/14/15 Pct Recovery = 108% Analysis Date = 12/09/15 Pct Recovery = 108% Analysis Date = 12/09/15 Pct Recovery = 108% Analysis Date = 12/05/15 Pct Recovery = 109% Analysis Date = 12/05/15 Pct Recovery = 109% Analysis Date = 11/30/15 Pct Recovery = 109% Analysis Date = 11/30/15 Pct Recovery = 109% Analysis Date = 11/25/15 Pct Recovery = 109% Analysis Date = 11/25/15 Pct Recovery = 109% Analysis Date = 11/20/15 Pct Recovery = 109% Analysis Date = 11/20/15 Pct Recovery = 109% Analysis Date = 11/16/15 Pct Recovery = 109% Analysis Date = 11/16/15 Pct Recovery = 109% Analysis Date = 11/11/15 Pct Recovery = 109% Analysis Date = 11/11/15 Pct Recovery = 109% Analysis Date = 11/06/15 Pct Recovery = 109% Analysis Date = 11/06/15 Pct Recovery = 109% Analysis Date = 11/01/15 Pct Recovery = 109% Analysis Date = 11/01/15 Pct Recovery = 109% Analysis Date = 10/27/15 Pct Recovery = 109% Analysis Date = 10/27/15 Pct Recovery = 109% Analysis Date = 10/23/15 Pct Recovery = 109% Analysis Date = 10/23/15 Pct Recovery = 109% Analysis Date = 10/18/15 Pct Recovery = 109% Analysis Date = 10/18/15 Pct Recovery = 109% Analysis Date = 10/13/15 Pct Recovery = 109% Analysis Date = 10/13/15 Pct Recovery = 109% Analysis Date = 10/08/15 Pct Recovery = 109% Analysis Date = 10/08/15 Pct Recovery = 109% Analysis Date = 10/04/15 Pct Recovery = 109% Analysis Date = 10/04/15 Pct Recovery = 109% Analysis Date = 09/29/15 Pct Recovery = 109% Analysis Date = 09/29/15 Pct Recovery = 109% Analysis Date = 09/24/15 Pct Recovery = 109% Analysis Date = 09/24/15 Pct Recovery = 109% Analysis Date = 09/19/15 Pct Recovery = 109% Analysis Date = 09/19/15 Pct Recovery = 109% Analysis Date = 09/14/15 Pct Recovery = 109% Analysis Date = 09/14/15 Pct Recovery = 109% Analysis Date = 09/10/15 Pct Recovery = 109% Analysis Date = 09/10/15 Pct Recovery = 109% Analysis Date = 09/05/15 Pct Recovery = 109% Analysis Date = 09/05/15 Pct Recovery = 109% Analysis Date = 08/31/15 Pct Recovery = 108% Analysis Date = 08/31/15 Pct Recovery = 108% Analysis Date = 08/26/15 Pct Recovery = 108% Analysis Date = 08/26/15 Pct Recovery = 108% Analysis Date = 08/21/15 Pct Recovery = 108% Analysis Date = 08/21/15 Pct Recovery = 108% Analysis Date = 08/17/15 Pct Recovery = 108% Analysis Date = 08/17/15 Pct Recovery = 108% Analysis Date = 08/12/15 Pct Recovery = 108% Analysis Date = 08/12/15 Pct Recovery = 108% Analysis Date = 08/07/15 Pct Recovery = 108% Analysis Date = 08/07/15 Pct Recovery = 108% Analysis Date = 08/02/15 Pct Recovery = 108% Analysis Date = 08/02/15 Pct Recovery = 108% Analysis Date = 07/29/15 Pct Recovery = 108% Analysis Date = 07/29/15 Pct Recovery = 108% Analysis Date = 07/24/15 Pct Recovery = 108% Analysis Date = 07/24/15 Pct Recovery = 108% Analysis Date = 07/19/15 Pct Recovery = 107% Analysis Date = 07/19/15 Pct Recovery = 107% Analysis Date = 07/14/15 Pct Recovery = 107% Analysis Date = 07/14/15 Pct Recovery = 107% Analysis Date = 07/09/15 Pct Recovery = 107% Analysis Date = 07/09/15 Pct Recovery = 107% Analysis Date = 07/05/15 Pct Recovery = 107% Analysis Date = 07/05/15 Pct Recovery = 107% Analysis Date = 06/30/15 Pct Recovery = 107% Analysis Date = 06/30/15 Pct Recovery = 107% Analysis Date = 06/25/15 Pct Recovery = 107% Analysis Date = 06/25/15 Pct Recovery = 107% Analysis Date = 06/20/15 Pct Recovery = 107% Analysis Date = 06/20/15 Pct Recovery = 107% Analysis Date = 06/16/15 Pct Recovery = 106% Analysis Date = 06/16/15 Pct Recovery = 106% Analysis Date = 06/11/15 Pct Recovery = 106% Analysis Date = 06/11/15 Pct Recovery = 106% Analysis Date = 06/06/15 Pct Recovery = 106% Analysis Date = 06/06/15 Pct Recovery = 106% Analysis Date = 06/01/15 Pct Recovery = 106% Analysis Date = 06/01/15 Pct Recovery = 106% Analysis Date = 05/27/15 Pct Recovery = 106% Analysis Date = 05/27/15 Pct Recovery = 106% Analysis Date = 05/23/15 Pct Recovery = 106% Analysis Date = 05/23/15 Pct Recovery = 106% Analysis Date = 05/18/15 Pct Recovery = 106% Analysis Date = 05/18/15 Pct Recovery = 106% Analysis Date = 05/13/15 Pct Recovery = 106% Analysis Date = 05/13/15 Pct Recovery = 106% Analysis Date = 05/08/15 Pct Recovery = 105% Analysis Date = 05/08/15 Pct Recovery = 105% Analysis Date = 05/04/15 Pct Recovery = 105% Analysis Date = 05/04/15 Pct Recovery = 105% Analysis Date = 04/29/15 Pct Recovery = 105% Analysis Date = 04/29/15 Pct Recovery = 105% Analysis Date = 04/24/15 Pct Recovery = 105% Analysis Date = 04/24/15 Pct Recovery = 105% Analysis Date = 04/19/15 Pct Recovery = 105% Analysis Date = 04/19/15 Pct Recovery = 105% Analysis Date = 04/14/15 Pct Recovery = 105% Analysis Date = 04/14/15 Pct Recovery = 105% Analysis Date = 04/10/15 Pct Recovery = 105% Analysis Date = 04/10/15 Pct Recovery = 105% Analysis Date = 04/05/15 Pct Recovery = 105% Analysis Date = 04/05/15 Pct Recovery = 105% Analysis Date = 03/31/15 Pct Recovery = 104% Analysis Date = 03/31/15 Pct Recovery = 104% Analysis Date = 03/26/15 Pct Recovery = 104% Analysis Date = 03/26/15 Pct Recovery = 104% Analysis Date = 03/22/15 Pct Recovery = 104% Analysis Date = 03/22/15 Pct Recovery = 104% Analysis Date = 03/17/15 Pct Recovery = 104% Analysis Date = 03/17/15 Pct Recovery = 104% Analysis Date = 03/12/15 Pct Recovery = 104% Analysis Date = 03/12/15 Pct Recovery = 104% Analysis Date = 03/07/15 Pct Recovery = 104% Analysis Date = 03/07/15 Pct Recovery = 104% Analysis Date = 03/02/15 Pct Recovery = 104% Analysis Date = 03/02/15 Pct Recovery = 104% Analysis Date = 02/26/15 Pct Recovery = 104% Analysis Date = 02/26/15 Pct Recovery = 104% Analysis Date = 02/21/15 Pct Recovery = 104% Analysis Date = 02/21/15 Pct Recovery = 104% Analysis Date = 02/16/15 Pct Recovery = 103% Analysis Date = 02/16/15 Pct Recovery = 103% Analysis Date = 02/11/15 Pct Recovery = 103% Analysis Date = 02/11/15 Pct Recovery = 103% Analysis Date = 02/07/15 Pct Recovery = 103% Analysis Date = 02/07/15 Pct Recovery = 103% Analysis Date = 02/02/15 Pct Recovery = 103% Analysis Date = 02/02/15 Pct Recovery = 103% Analysis Date = 01/28/15 Pct Recovery = 103% Analysis Date = 01/28/15 Pct Recovery = 103% Analysis Date = 01/23/15 Pct Recovery = 103% Analysis Date = 01/23/15 Pct Recovery = 103% Analysis Date = 01/18/15 Pct Recovery = 103% Analysis Date = 01/18/15 Pct Recovery = 103% Analysis Date = 01/14/15 Pct Recovery = 103% Analysis Date = 01/14/15 Pct Recovery = 103% Analysis Date = 01/09/15 Pct Recovery = 102% Analysis Date = 01/09/15 Pct Recovery = 102% Analysis Date = 01/04/15 Pct Recovery = 102% Analysis Date = 01/04/15 Pct Recovery = 102% Analysis Date = 12/30/14 Pct Recovery = 102% Analysis Date = 12/30/14 Pct Recovery = 102% Analysis Date = 12/25/14 Pct Recovery = 102% Analysis Date = 12/25/14 Pct Recovery = 102% Analysis Date = 12/21/14 Pct Recovery = 102% Analysis Date = 12/21/14 Pct Recovery = 102% Analysis Date = 12/16/14 Pct Recovery = 102% Analysis Date = 12/16/14 Pct Recovery = 102% Analysis Date = 12/11/14 Pct Recovery = 102% Analysis Date = 12/11/14 Pct Recovery = 102% Analysis Date = 12/06/14 Pct Recovery = 102% Analysis Date = 12/06/14 Pct Recovery = 102% Analysis Date = 12/02/14 Pct Recovery = 101% Analysis Date = 12/02/14 Pct Recovery = 101% Analysis Date = 11/27/14 Pct Recovery = 101% Analysis Date = 11/27/14 Pct Recovery = 101% Analysis Date = 11/22/14 Pct Recovery = 101% Analysis Date = 11/22/14 Pct Recovery = 101% Analysis Date = 11/17/14 Pct Recovery = 101% Analysis Date = 11/17/14 Pct Recovery = 101% Analysis Date = 11/12/14 Pct Recovery = 101% Analysis Date = 11/12/14 Pct Recovery = 101% Analysis Date = 11/08/14 Pct Recovery = 101% Analysis Date = 11/08/14 Pct Recovery = 101% Analysis Date = 11/03/14 Pct Recovery = 101% Analysis Date = 11/03/14 Pct Recovery = 101% Analysis Date = 10/29/14 Pct Recovery = 101% Analysis Date = 10/29/14 Pct Recovery = 101% Analysis Date = 10/24/14 Pct Recovery = 100% Analysis Date = 10/24/14 Pct Recovery = 100% Analysis Date = 10/20/14 Pct Recovery = 100% Analysis Date = 10/20/14 Pct Recovery = 100% Analysis Date = 10/15/14 Pct Recovery = 100% Analysis Date = 10/15/14 Pct Recovery = 100% Analysis Date = 10/10/14 Pct Recovery = 100% Analysis Date = 10/10/14 Pct Recovery = 100% Analysis Date = 10/05/14 Pct Recovery = 100% Analysis Date = 10/05/14 Pct Recovery = 100% Analysis Date = 09/30/14 Pct Recovery = 100% Analysis Date = 09/30/14 Pct Recovery = 100% Analysis Date = 09/26/14 Pct Recovery = 100% Analysis Date = 09/26/14 Pct Recovery = 100% Analysis Date = 09/21/14 Pct Recovery = 99% Analysis Date = 09/21/14 Pct Recovery = 99% Analysis Date = 09/16/14 Pct Recovery = 99% Analysis Date = 09/16/14 Pct Recovery = 99% Analysis Date = 09/11/14 Pct Recovery = 99% Analysis Date = 09/11/14 Pct Recovery = 99% Analysis Date = 09/07/14 Pct Recovery = 99% Analysis Date = 09/07/14 Pct Recovery = 99% Analysis Date = 09/02/14 Pct Recovery = 99% Analysis Date = 09/02/14 Pct Recovery = 99% Analysis Date = 08/28/14 Pct Recovery = 99% Analysis Date = 08/28/14 Pct Recovery = 99% Analysis Date = 08/23/14 Pct Recovery = 99% Analysis Date = 08/23/14 Pct Recovery = 99% Analysis Date = 08/18/14 Pct Recovery = 99% Analysis Date = 08/18/14 Pct Recovery = 99% Analysis Date = 08/14/14 Pct Recovery = 98% Analysis Date = 08/14/14 Pct Recovery = 98% Analysis Date = 08/09/14 Pct Recovery = 98% Analysis Date = 08/09/14 Pct Recovery = 98% Analysis Date = 08/04/14 Pct Recovery = 98% Analysis Date = 08/04/14 Pct Recovery = 98% Analysis Date = 07/30/14 Pct Recovery = 98% Analysis Date = 07/30/14 Pct Recovery = 98% Analysis Date = 07/26/14 Pct Recovery = 98% Analysis Date = 07/26/14 Pct Recovery = 98% Analysis Date = 07/21/14 Pct Recovery = 98% Analysis Date = 07/21/14 Pct Recovery = 98% Analysis Date = 07/16/14 Pct Recovery = 98% Analysis Date = 07/16/14 Pct Recovery = 98% Analysis Date = 07/11/14 Pct Recovery = 97% Analysis Date = 07/11/14 Pct Recovery = 97% Analysis Date = 07/06/14 Pct Recovery = 97% Analysis Date = 07/06/14 Pct Recovery = 97% Analysis Date = 07/02/14 Pct Recovery = 97% Analysis Date = 07/02/14 Pct Recovery = 97% Analysis Date = 06/27/14 Pct Recovery = 97% Analysis Date = 06/27/14 Pct Recovery = 97% Analysis Date = 06/22/14 Pct Recovery = 97% Analysis Date = 06/22/14 Pct Recovery = 97% Analysis Date = 06/17/14 Pct Recovery = 97% Analysis Date = 06/17/14 Pct Recovery = 97% Analysis Date = 06/13/14 Pct Recovery = 97% Analysis Date = 06/13/14 Pct Recovery = 97% Analysis Date = 06/08/14 Pct Recovery = 97% Analysis Date = 06/08/14 Pct Recovery = 97% Analysis Date = 06/03/14 Pct Recovery = 96% Analysis Date = 06/03/14 Pct Recovery = 96% Analysis Date = 05/29/14 Pct Recovery = 96% Analysis Date = 05/29/14 Pct Recovery = 96% Analysis Date = 05/24/14 Pct Recovery = 96% Analysis Date = 05/24/14 Pct Recovery = 96% Analysis Date = 05/20/14 Pct Recovery = 96% Analysis Date = 05/20/14 Pct Recovery = 96% Analysis Date = 05/15/14 Pct Recovery = 96% Analysis Date = 05/15/14 Pct Recovery = 96% Analysis Date = 05/10/14 Pct Recovery = 96% Analysis Date = 05/10/14 Pct Recovery = 96% Analysis Date = 05/05/14 Pct Recovery = 96% Analysis Date = 05/05/14 Pct Recovery = 96% Analysis Date = 05/01/14 Pct Recovery = 95% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
1,2-DIBROMOETHANE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 48 102% 14% 100% 11%
Total 48 102% 14% 100% 11%

Sample Statistics
1,2-DIBROMOETHANE

Characteristic N % % Basis
Plotted 48 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 48 .  
False Negatives 0 0% 0 out of 48
Not Spiked 25 .  
False Positives 0 0% 0 out of 25

BQS OBSP Determination:
1,2-DICHLORO-1,1,2,2-TETRAFLUOROETHANE
METHOD: 4440 , TESTIDCODE: 50985GCM66
Open Data Set

Analysis Date = 12/12/16 SpikeMix = Accu 216041125: 40 µl & Crescent 03FF058: 40 µl Pct Recovery = 54% Analysis Date = 08/04/16 SpikeMix = Crescent 03FF058: 40 µl & Supelco LC20141V: 40 µl Pct Recovery = 56% Analysis Date = 11/21/16 SpikeMix = Crescent 03FF058: 25 µl & Supelco LC20141V: 25 µl Pct Recovery = 51% Analysis Date = 06/30/16 SpikeMix = Crescent 03FF058: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 60% Analysis Date = 06/21/16 SpikeMix = Phenova B20160319: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 55% Analysis Date = 05/24/16 SpikeMix = Accu 216041125: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 55% Analysis Date = 08/15/15 SpikeMix = Supelco LC13545: 25 µl & Crescent 04EE008: 25 µl Pct Recovery = 123% Analysis Date = 06/16/15 SpikeMix = ERA 0406-15-03: 25 µl & Supelco LC13545: 25 µl Pct Recovery = 122% Analysis Date = 09/28/16 SpikeMix = Crescent 03FF058: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 63% Analysis Date = 09/08/16 SpikeMix = Phenova B20160319: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 57% Analysis Date = 08/20/16 SpikeMix = Accu 216041125: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 57% Analysis Date = 04/26/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 43% Analysis Date = 02/05/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 75% Analysis Date = 11/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 72% Analysis Date = 10/16/15 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 74% Analysis Date = 05/09/15 SpikeMix = Spex Organics EN150428007: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 92% Analysis Date = 04/02/16 SpikeMix = Supelco LC13545: 15 µl & Accu 215041380: 15 µl Pct Recovery = 143% Analysis Date = 12/18/15 SpikeMix = Supelco LC13545: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 127% Analysis Date = 02/18/16 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 80% Analysis Date = 11/12/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 75% Analysis Date = 09/03/15 SpikeMix = NSI 050515AVOC: 10 µl & Spex Organics EN150428007: 10 µl Pct Recovery = 84% Analysis Date = 05/21/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 98% Analysis Date = 05/13/16 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 90% Analysis Date = 03/17/16 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 126% Analysis Date = 12/10/15 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 151% Analysis Date = 06/27/15 SpikeMix = ERA 0406-15-03: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 110% Analysis Date = 05/09/15 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 140% Analysis Date = 12/12/16 Pct Recovery = 47% Analysis Date = 12/09/16 Pct Recovery = 47% Analysis Date = 12/09/16 Pct Recovery = 47% Analysis Date = 12/06/16 Pct Recovery = 48% Analysis Date = 12/06/16 Pct Recovery = 48% Analysis Date = 12/03/16 Pct Recovery = 48% Analysis Date = 12/03/16 Pct Recovery = 48% Analysis Date = 11/30/16 Pct Recovery = 48% Analysis Date = 11/30/16 Pct Recovery = 48% Analysis Date = 11/27/16 Pct Recovery = 49% Analysis Date = 11/27/16 Pct Recovery = 49% Analysis Date = 11/24/16 Pct Recovery = 49% Analysis Date = 11/24/16 Pct Recovery = 49% Analysis Date = 11/21/16 Pct Recovery = 49% Analysis Date = 11/21/16 Pct Recovery = 49% Analysis Date = 11/18/16 Pct Recovery = 50% Analysis Date = 11/18/16 Pct Recovery = 50% Analysis Date = 11/15/16 Pct Recovery = 50% Analysis Date = 11/15/16 Pct Recovery = 50% Analysis Date = 11/12/16 Pct Recovery = 50% Analysis Date = 11/12/16 Pct Recovery = 50% Analysis Date = 11/09/16 Pct Recovery = 51% Analysis Date = 11/09/16 Pct Recovery = 51% Analysis Date = 11/07/16 Pct Recovery = 51% Analysis Date = 11/07/16 Pct Recovery = 51% Analysis Date = 11/04/16 Pct Recovery = 51% Analysis Date = 11/04/16 Pct Recovery = 51% Analysis Date = 11/01/16 Pct Recovery = 52% Analysis Date = 11/01/16 Pct Recovery = 52% Analysis Date = 10/29/16 Pct Recovery = 52% Analysis Date = 10/29/16 Pct Recovery = 52% Analysis Date = 10/26/16 Pct Recovery = 52% Analysis Date = 10/26/16 Pct Recovery = 52% Analysis Date = 10/23/16 Pct Recovery = 53% Analysis Date = 10/23/16 Pct Recovery = 53% Analysis Date = 10/20/16 Pct Recovery = 53% Analysis Date = 10/20/16 Pct Recovery = 53% Analysis Date = 10/17/16 Pct Recovery = 54% Analysis Date = 10/17/16 Pct Recovery = 54% Analysis Date = 10/14/16 Pct Recovery = 54% Analysis Date = 10/14/16 Pct Recovery = 54% Analysis Date = 10/11/16 Pct Recovery = 54% Analysis Date = 10/11/16 Pct Recovery = 54% Analysis Date = 10/08/16 Pct Recovery = 55% Analysis Date = 10/08/16 Pct Recovery = 55% Analysis Date = 10/05/16 Pct Recovery = 55% Analysis Date = 10/05/16 Pct Recovery = 55% Analysis Date = 10/03/16 Pct Recovery = 55% Analysis Date = 10/03/16 Pct Recovery = 55% Analysis Date = 09/30/16 Pct Recovery = 56% Analysis Date = 09/30/16 Pct Recovery = 56% Analysis Date = 09/27/16 Pct Recovery = 56% Analysis Date = 09/27/16 Pct Recovery = 56% Analysis Date = 09/24/16 Pct Recovery = 56% Analysis Date = 09/24/16 Pct Recovery = 56% Analysis Date = 09/21/16 Pct Recovery = 57% Analysis Date = 09/21/16 Pct Recovery = 57% Analysis Date = 09/18/16 Pct Recovery = 57% Analysis Date = 09/18/16 Pct Recovery = 57% Analysis Date = 09/15/16 Pct Recovery = 57% Analysis Date = 09/15/16 Pct Recovery = 57% Analysis Date = 09/12/16 Pct Recovery = 58% Analysis Date = 09/12/16 Pct Recovery = 58% Analysis Date = 09/09/16 Pct Recovery = 58% Analysis Date = 09/09/16 Pct Recovery = 58% Analysis Date = 09/06/16 Pct Recovery = 58% Analysis Date = 09/06/16 Pct Recovery = 58% Analysis Date = 09/03/16 Pct Recovery = 59% Analysis Date = 09/03/16 Pct Recovery = 59% Analysis Date = 08/31/16 Pct Recovery = 59% Analysis Date = 08/31/16 Pct Recovery = 59% Analysis Date = 08/29/16 Pct Recovery = 60% Analysis Date = 08/29/16 Pct Recovery = 60% Analysis Date = 08/26/16 Pct Recovery = 60% Analysis Date = 08/26/16 Pct Recovery = 60% Analysis Date = 08/23/16 Pct Recovery = 60% Analysis Date = 08/23/16 Pct Recovery = 60% Analysis Date = 08/20/16 Pct Recovery = 61% Analysis Date = 08/20/16 Pct Recovery = 61% Analysis Date = 08/17/16 Pct Recovery = 61% Analysis Date = 08/17/16 Pct Recovery = 61% Analysis Date = 08/14/16 Pct Recovery = 62% Analysis Date = 08/14/16 Pct Recovery = 62% Analysis Date = 08/11/16 Pct Recovery = 62% Analysis Date = 08/11/16 Pct Recovery = 62% Analysis Date = 08/08/16 Pct Recovery = 62% Analysis Date = 08/08/16 Pct Recovery = 62% Analysis Date = 08/05/16 Pct Recovery = 63% Analysis Date = 08/05/16 Pct Recovery = 63% Analysis Date = 08/02/16 Pct Recovery = 63% Analysis Date = 08/02/16 Pct Recovery = 63% Analysis Date = 07/30/16 Pct Recovery = 64% Analysis Date = 07/30/16 Pct Recovery = 64% Analysis Date = 07/27/16 Pct Recovery = 64% Analysis Date = 07/27/16 Pct Recovery = 64% Analysis Date = 07/25/16 Pct Recovery = 64% Analysis Date = 07/25/16 Pct Recovery = 64% Analysis Date = 07/22/16 Pct Recovery = 65% Analysis Date = 07/22/16 Pct Recovery = 65% Analysis Date = 07/19/16 Pct Recovery = 65% Analysis Date = 07/19/16 Pct Recovery = 65% Analysis Date = 07/16/16 Pct Recovery = 66% Analysis Date = 07/16/16 Pct Recovery = 66% Analysis Date = 07/13/16 Pct Recovery = 66% Analysis Date = 07/13/16 Pct Recovery = 66% Analysis Date = 07/10/16 Pct Recovery = 66% Analysis Date = 07/10/16 Pct Recovery = 66% Analysis Date = 07/07/16 Pct Recovery = 67% Analysis Date = 07/07/16 Pct Recovery = 67% Analysis Date = 07/04/16 Pct Recovery = 67% Analysis Date = 07/04/16 Pct Recovery = 67% Analysis Date = 07/01/16 Pct Recovery = 68% Analysis Date = 07/01/16 Pct Recovery = 68% Analysis Date = 06/28/16 Pct Recovery = 68% Analysis Date = 06/28/16 Pct Recovery = 68% Analysis Date = 06/25/16 Pct Recovery = 69% Analysis Date = 06/25/16 Pct Recovery = 69% Analysis Date = 06/23/16 Pct Recovery = 69% Analysis Date = 06/23/16 Pct Recovery = 69% Analysis Date = 06/20/16 Pct Recovery = 70% Analysis Date = 06/20/16 Pct Recovery = 70% Analysis Date = 06/17/16 Pct Recovery = 71% Analysis Date = 06/17/16 Pct Recovery = 71% Analysis Date = 06/14/16 Pct Recovery = 71% Analysis Date = 06/14/16 Pct Recovery = 71% Analysis Date = 06/11/16 Pct Recovery = 72% Analysis Date = 06/11/16 Pct Recovery = 72% Analysis Date = 06/08/16 Pct Recovery = 72% Analysis Date = 06/08/16 Pct Recovery = 72% Analysis Date = 06/05/16 Pct Recovery = 73% Analysis Date = 06/05/16 Pct Recovery = 73% Analysis Date = 06/02/16 Pct Recovery = 74% Analysis Date = 06/02/16 Pct Recovery = 74% Analysis Date = 05/30/16 Pct Recovery = 74% Analysis Date = 05/30/16 Pct Recovery = 74% Analysis Date = 05/27/16 Pct Recovery = 75% Analysis Date = 05/27/16 Pct Recovery = 75% Analysis Date = 05/24/16 Pct Recovery = 75% Analysis Date = 05/24/16 Pct Recovery = 75% Analysis Date = 05/21/16 Pct Recovery = 76% Analysis Date = 05/21/16 Pct Recovery = 76% Analysis Date = 05/19/16 Pct Recovery = 77% Analysis Date = 05/19/16 Pct Recovery = 77% Analysis Date = 05/16/16 Pct Recovery = 77% Analysis Date = 05/16/16 Pct Recovery = 77% Analysis Date = 05/13/16 Pct Recovery = 78% Analysis Date = 05/13/16 Pct Recovery = 78% Analysis Date = 05/10/16 Pct Recovery = 79% Analysis Date = 05/10/16 Pct Recovery = 79% Analysis Date = 05/07/16 Pct Recovery = 79% Analysis Date = 05/07/16 Pct Recovery = 79% Analysis Date = 05/04/16 Pct Recovery = 80% Analysis Date = 05/04/16 Pct Recovery = 80% Analysis Date = 05/01/16 Pct Recovery = 81% Analysis Date = 05/01/16 Pct Recovery = 81% Analysis Date = 04/28/16 Pct Recovery = 82% Analysis Date = 04/28/16 Pct Recovery = 82% Analysis Date = 04/25/16 Pct Recovery = 82% Analysis Date = 04/25/16 Pct Recovery = 82% Analysis Date = 04/22/16 Pct Recovery = 83% Analysis Date = 04/22/16 Pct Recovery = 83% Analysis Date = 04/19/16 Pct Recovery = 84% Analysis Date = 04/19/16 Pct Recovery = 84% Analysis Date = 04/16/16 Pct Recovery = 85% Analysis Date = 04/16/16 Pct Recovery = 85% Analysis Date = 04/14/16 Pct Recovery = 86% Analysis Date = 04/14/16 Pct Recovery = 86% Analysis Date = 04/11/16 Pct Recovery = 86% Analysis Date = 04/11/16 Pct Recovery = 86% Analysis Date = 04/08/16 Pct Recovery = 87% Analysis Date = 04/08/16 Pct Recovery = 87% Analysis Date = 04/05/16 Pct Recovery = 88% Analysis Date = 04/05/16 Pct Recovery = 88% Analysis Date = 04/02/16 Pct Recovery = 89% Analysis Date = 04/02/16 Pct Recovery = 89% Analysis Date = 03/30/16 Pct Recovery = 89% Analysis Date = 03/30/16 Pct Recovery = 89% Analysis Date = 03/27/16 Pct Recovery = 90% Analysis Date = 03/27/16 Pct Recovery = 90% Analysis Date = 03/24/16 Pct Recovery = 90% Analysis Date = 03/24/16 Pct Recovery = 90% Analysis Date = 03/21/16 Pct Recovery = 91% Analysis Date = 03/21/16 Pct Recovery = 91% Analysis Date = 03/18/16 Pct Recovery = 91% Analysis Date = 03/18/16 Pct Recovery = 91% Analysis Date = 03/15/16 Pct Recovery = 92% Analysis Date = 03/15/16 Pct Recovery = 92% Analysis Date = 03/12/16 Pct Recovery = 92% Analysis Date = 03/12/16 Pct Recovery = 92% Analysis Date = 03/10/16 Pct Recovery = 93% Analysis Date = 03/10/16 Pct Recovery = 93% Analysis Date = 03/07/16 Pct Recovery = 93% Analysis Date = 03/07/16 Pct Recovery = 93% Analysis Date = 03/04/16 Pct Recovery = 94% Analysis Date = 03/04/16 Pct Recovery = 94% Analysis Date = 03/01/16 Pct Recovery = 94% Analysis Date = 03/01/16 Pct Recovery = 94% Analysis Date = 02/27/16 Pct Recovery = 95% Analysis Date = 02/27/16 Pct Recovery = 95% Analysis Date = 02/24/16 Pct Recovery = 95% Analysis Date = 02/24/16 Pct Recovery = 95% Analysis Date = 02/21/16 Pct Recovery = 96% Analysis Date = 02/21/16 Pct Recovery = 96% Analysis Date = 02/18/16 Pct Recovery = 96% Analysis Date = 02/18/16 Pct Recovery = 96% Analysis Date = 02/15/16 Pct Recovery = 96% Analysis Date = 02/15/16 Pct Recovery = 96% Analysis Date = 02/12/16 Pct Recovery = 96% Analysis Date = 02/12/16 Pct Recovery = 96% Analysis Date = 02/09/16 Pct Recovery = 97% Analysis Date = 02/09/16 Pct Recovery = 97% Analysis Date = 02/07/16 Pct Recovery = 97% Analysis Date = 02/07/16 Pct Recovery = 97% Analysis Date = 02/04/16 Pct Recovery = 97% Analysis Date = 02/04/16 Pct Recovery = 97% Analysis Date = 02/01/16 Pct Recovery = 97% Analysis Date = 02/01/16 Pct Recovery = 97% Analysis Date = 01/29/16 Pct Recovery = 97% Analysis Date = 01/29/16 Pct Recovery = 97% Analysis Date = 01/26/16 Pct Recovery = 97% Analysis Date = 01/26/16 Pct Recovery = 97% Analysis Date = 01/23/16 Pct Recovery = 97% Analysis Date = 01/23/16 Pct Recovery = 97% Analysis Date = 01/20/16 Pct Recovery = 97% Analysis Date = 01/20/16 Pct Recovery = 97% Analysis Date = 01/17/16 Pct Recovery = 97% Analysis Date = 01/17/16 Pct Recovery = 97% Analysis Date = 01/14/16 Pct Recovery = 97% Analysis Date = 01/14/16 Pct Recovery = 97% Analysis Date = 01/11/16 Pct Recovery = 97% Analysis Date = 01/11/16 Pct Recovery = 97% Analysis Date = 01/08/16 Pct Recovery = 97% Analysis Date = 01/08/16 Pct Recovery = 97% Analysis Date = 01/05/16 Pct Recovery = 97% Analysis Date = 01/05/16 Pct Recovery = 97% Analysis Date = 01/03/16 Pct Recovery = 97% Analysis Date = 01/03/16 Pct Recovery = 97% Analysis Date = 12/31/15 Pct Recovery = 97% Analysis Date = 12/31/15 Pct Recovery = 97% Analysis Date = 12/28/15 Pct Recovery = 97% Analysis Date = 12/28/15 Pct Recovery = 97% Analysis Date = 12/25/15 Pct Recovery = 98% Analysis Date = 12/25/15 Pct Recovery = 98% Analysis Date = 12/22/15 Pct Recovery = 98% Analysis Date = 12/22/15 Pct Recovery = 98% Analysis Date = 12/19/15 Pct Recovery = 98% Analysis Date = 12/19/15 Pct Recovery = 98% Analysis Date = 12/16/15 Pct Recovery = 98% Analysis Date = 12/16/15 Pct Recovery = 98% Analysis Date = 12/13/15 Pct Recovery = 98% Analysis Date = 12/13/15 Pct Recovery = 98% Analysis Date = 12/10/15 Pct Recovery = 98% Analysis Date = 12/10/15 Pct Recovery = 98% Analysis Date = 12/07/15 Pct Recovery = 98% Analysis Date = 12/07/15 Pct Recovery = 98% Analysis Date = 12/04/15 Pct Recovery = 98% Analysis Date = 12/04/15 Pct Recovery = 98% Analysis Date = 12/01/15 Pct Recovery = 98% Analysis Date = 12/01/15 Pct Recovery = 98% Analysis Date = 11/29/15 Pct Recovery = 98% Analysis Date = 11/29/15 Pct Recovery = 98% Analysis Date = 11/26/15 Pct Recovery = 98% Analysis Date = 11/26/15 Pct Recovery = 98% Analysis Date = 11/23/15 Pct Recovery = 98% Analysis Date = 11/23/15 Pct Recovery = 98% Analysis Date = 11/20/15 Pct Recovery = 98% Analysis Date = 11/20/15 Pct Recovery = 98% Analysis Date = 11/17/15 Pct Recovery = 98% Analysis Date = 11/17/15 Pct Recovery = 98% Analysis Date = 11/14/15 Pct Recovery = 98% Analysis Date = 11/14/15 Pct Recovery = 98% Analysis Date = 11/11/15 Pct Recovery = 98% Analysis Date = 11/11/15 Pct Recovery = 98% Analysis Date = 11/08/15 Pct Recovery = 98% Analysis Date = 11/08/15 Pct Recovery = 98% Analysis Date = 11/05/15 Pct Recovery = 98% Analysis Date = 11/05/15 Pct Recovery = 98% Analysis Date = 11/02/15 Pct Recovery = 98% Analysis Date = 11/02/15 Pct Recovery = 98% Analysis Date = 10/30/15 Pct Recovery = 99% Analysis Date = 10/30/15 Pct Recovery = 99% Analysis Date = 10/27/15 Pct Recovery = 99% Analysis Date = 10/27/15 Pct Recovery = 99% Analysis Date = 10/25/15 Pct Recovery = 99% Analysis Date = 10/25/15 Pct Recovery = 99% Analysis Date = 10/22/15 Pct Recovery = 99% Analysis Date = 10/22/15 Pct Recovery = 99% Analysis Date = 10/19/15 Pct Recovery = 99% Analysis Date = 10/19/15 Pct Recovery = 99% Analysis Date = 10/16/15 Pct Recovery = 100% Analysis Date = 10/16/15 Pct Recovery = 100% Analysis Date = 10/13/15 Pct Recovery = 100% Analysis Date = 10/13/15 Pct Recovery = 100% Analysis Date = 10/10/15 Pct Recovery = 100% Analysis Date = 10/10/15 Pct Recovery = 100% Analysis Date = 10/07/15 Pct Recovery = 100% Analysis Date = 10/07/15 Pct Recovery = 100% Analysis Date = 10/04/15 Pct Recovery = 100% Analysis Date = 10/04/15 Pct Recovery = 100% Analysis Date = 10/01/15 Pct Recovery = 101% Analysis Date = 10/01/15 Pct Recovery = 101% Analysis Date = 09/28/15 Pct Recovery = 101% Analysis Date = 09/28/15 Pct Recovery = 101% Analysis Date = 09/25/15 Pct Recovery = 101% Analysis Date = 09/25/15 Pct Recovery = 101% Analysis Date = 09/23/15 Pct Recovery = 101% Analysis Date = 09/23/15 Pct Recovery = 101% Analysis Date = 09/20/15 Pct Recovery = 101% Analysis Date = 09/20/15 Pct Recovery = 101% Analysis Date = 09/17/15 Pct Recovery = 102% Analysis Date = 09/17/15 Pct Recovery = 102% Analysis Date = 09/14/15 Pct Recovery = 102% Analysis Date = 09/14/15 Pct Recovery = 102% Analysis Date = 09/11/15 Pct Recovery = 102% Analysis Date = 09/11/15 Pct Recovery = 102% Analysis Date = 09/08/15 Pct Recovery = 102% Analysis Date = 09/08/15 Pct Recovery = 102% Analysis Date = 09/05/15 Pct Recovery = 102% Analysis Date = 09/05/15 Pct Recovery = 102% Analysis Date = 09/02/15 Pct Recovery = 103% Analysis Date = 09/02/15 Pct Recovery = 103% Analysis Date = 08/30/15 Pct Recovery = 103% Analysis Date = 08/30/15 Pct Recovery = 103% Analysis Date = 08/27/15 Pct Recovery = 103% Analysis Date = 08/27/15 Pct Recovery = 103% Analysis Date = 08/24/15 Pct Recovery = 103% Analysis Date = 08/24/15 Pct Recovery = 103% Analysis Date = 08/21/15 Pct Recovery = 104% Analysis Date = 08/21/15 Pct Recovery = 104% Analysis Date = 08/19/15 Pct Recovery = 104% Analysis Date = 08/19/15 Pct Recovery = 104% Analysis Date = 08/16/15 Pct Recovery = 104% Analysis Date = 08/16/15 Pct Recovery = 104% Analysis Date = 08/13/15 Pct Recovery = 104% Analysis Date = 08/13/15 Pct Recovery = 104% Analysis Date = 08/10/15 Pct Recovery = 105% Analysis Date = 08/10/15 Pct Recovery = 105% Analysis Date = 08/07/15 Pct Recovery = 105% Analysis Date = 08/07/15 Pct Recovery = 105% Analysis Date = 08/04/15 Pct Recovery = 105% Analysis Date = 08/04/15 Pct Recovery = 105% Analysis Date = 08/01/15 Pct Recovery = 105% Analysis Date = 08/01/15 Pct Recovery = 105% Analysis Date = 07/29/15 Pct Recovery = 105% Analysis Date = 07/29/15 Pct Recovery = 105% Analysis Date = 07/26/15 Pct Recovery = 106% Analysis Date = 07/26/15 Pct Recovery = 106% Analysis Date = 07/23/15 Pct Recovery = 106% Analysis Date = 07/23/15 Pct Recovery = 106% Analysis Date = 07/20/15 Pct Recovery = 106% Analysis Date = 07/20/15 Pct Recovery = 106% Analysis Date = 07/17/15 Pct Recovery = 106% Analysis Date = 07/17/15 Pct Recovery = 106% Analysis Date = 07/15/15 Pct Recovery = 107% Analysis Date = 07/15/15 Pct Recovery = 107% Analysis Date = 07/12/15 Pct Recovery = 107% Analysis Date = 07/12/15 Pct Recovery = 107% Analysis Date = 07/09/15 Pct Recovery = 107% Analysis Date = 07/09/15 Pct Recovery = 107% Analysis Date = 07/06/15 Pct Recovery = 107% Analysis Date = 07/06/15 Pct Recovery = 107% Analysis Date = 07/03/15 Pct Recovery = 108% Analysis Date = 07/03/15 Pct Recovery = 108% Analysis Date = 06/30/15 Pct Recovery = 108% Analysis Date = 06/30/15 Pct Recovery = 108% Analysis Date = 06/27/15 Pct Recovery = 108% Analysis Date = 06/27/15 Pct Recovery = 108% Analysis Date = 06/24/15 Pct Recovery = 108% Analysis Date = 06/24/15 Pct Recovery = 108% Analysis Date = 06/21/15 Pct Recovery = 109% Analysis Date = 06/21/15 Pct Recovery = 109% Analysis Date = 06/18/15 Pct Recovery = 109% Analysis Date = 06/18/15 Pct Recovery = 109% Analysis Date = 06/15/15 Pct Recovery = 109% Analysis Date = 06/15/15 Pct Recovery = 109% Analysis Date = 06/12/15 Pct Recovery = 109% Analysis Date = 06/12/15 Pct Recovery = 109% Analysis Date = 06/10/15 Pct Recovery = 110% Analysis Date = 06/10/15 Pct Recovery = 110% Analysis Date = 06/07/15 Pct Recovery = 110% Analysis Date = 06/07/15 Pct Recovery = 110% Analysis Date = 06/04/15 Pct Recovery = 110% Analysis Date = 06/04/15 Pct Recovery = 110% Analysis Date = 06/01/15 Pct Recovery = 111% Analysis Date = 06/01/15 Pct Recovery = 111% Analysis Date = 05/29/15 Pct Recovery = 111% Analysis Date = 05/29/15 Pct Recovery = 111% Analysis Date = 05/26/15 Pct Recovery = 111% Analysis Date = 05/26/15 Pct Recovery = 111% Analysis Date = 05/23/15 Pct Recovery = 112% Analysis Date = 05/23/15 Pct Recovery = 112% Analysis Date = 05/20/15 Pct Recovery = 112% Analysis Date = 05/20/15 Pct Recovery = 112% Analysis Date = 05/17/15 Pct Recovery = 112% Analysis Date = 05/17/15 Pct Recovery = 112% Analysis Date = 05/14/15 Pct Recovery = 112% Analysis Date = 05/14/15 Pct Recovery = 112% Analysis Date = 05/11/15 Pct Recovery = 113% Analysis Date = 05/11/15 Pct Recovery = 113% Analysis Date = 05/09/15 Pct Recovery = 113% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
1,2-DICHLORO-1,1,2,2-TETRAFLUOROETHANE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 27 86% 32% 75% 48%
Total 27 86% 32% 75% 48%

Sample Statistics
1,2-DICHLORO-1,1,2,2-TETRAFLUOROETHANE

Characteristic N % % Basis
Plotted 27 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 27 .  
False Negatives 0 0% 0 out of 27
Not Spiked 46 .  
False Positives 0 0% 0 out of 46

BQS OBSP Determination:
1,2-DICHLOROBENZENE
METHOD: 4440 , TESTIDCODE: 34536GCM66
Open Data Set

Analysis Date = 12/12/16 SpikeMix = Accu 216041125: 40 µl & Crescent 03FF058: 40 µl Pct Recovery = 100% Analysis Date = 08/04/16 SpikeMix = Crescent 03FF058: 40 µl & Supelco LC20141V: 40 µl Pct Recovery = 103% Analysis Date = 11/21/16 SpikeMix = Crescent 03FF058: 25 µl & Supelco LC20141V: 25 µl Pct Recovery = 96% Analysis Date = 06/30/16 SpikeMix = Crescent 03FF058: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 104% Analysis Date = 06/21/16 SpikeMix = Phenova B20160319: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 102% Analysis Date = 05/24/16 SpikeMix = Accu 216041125: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 90% Analysis Date = 03/06/15 SpikeMix = ERA 0227-14-06.1A: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 106% Analysis Date = 12/17/14 SpikeMix = Supelco LC06438: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 83% Analysis Date = 09/21/14 SpikeMix = Supelco LC06438: 20 µl Pct Recovery = 79% Analysis Date = 06/10/14 SpikeMix = NSI 032614: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 103% Analysis Date = 03/19/15 SpikeMix = Spex Organics C1140417015: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 104% Analysis Date = 11/22/14 SpikeMix = NSI 032614: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 117% Analysis Date = 08/19/14 SpikeMix = Spex Organics C1140417015: 20 µl & Accu 214031115: 20 µl Pct Recovery = 95% Analysis Date = 08/16/14 SpikeMix = ERA 0227-14-06.1A: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 107% Analysis Date = 09/29/15 SpikeMix = Accu 215041380: 25 µl & ERA 0406-15-03: 25 µl Pct Recovery = 97% Analysis Date = 06/16/15 SpikeMix = ERA 0406-15-03: 25 µl & Supelco LC13545: 25 µl Pct Recovery = 96% Analysis Date = 07/13/15 SpikeMix = Crescent 04EE008: 25 µl & NSI 050515AVOC: 25 µl Pct Recovery = 79% Analysis Date = 09/28/16 SpikeMix = Crescent 03FF058: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 92% Analysis Date = 09/08/16 SpikeMix = Phenova B20160319: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 87% Analysis Date = 08/20/16 SpikeMix = Accu 216041125: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 92% Analysis Date = 04/26/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 104% Analysis Date = 03/04/16 SpikeMix = Accu 215041380: 15 µl & ERA 0406-15-03: 15 µl Pct Recovery = 88% Analysis Date = 02/05/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 87% Analysis Date = 10/16/15 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 100% Analysis Date = 11/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 92% Analysis Date = 10/17/15 SpikeMix = Crescent 04EE008: 15 µl & NSI 050515AVOC: 15 µl Pct Recovery = 87% Analysis Date = 06/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Accu 215041380: 15 µl Pct Recovery = 88% Analysis Date = 10/21/14 SpikeMix = ERA 0227-14-06.1A: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 97% Analysis Date = 06/18/14 SpikeMix = Supelco LC06438: 10 µl & Accu 214031115: 10 µl Pct Recovery = 86% Analysis Date = 05/30/14 SpikeMix = NSI 032614: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 76% Analysis Date = 05/03/14 SpikeMix = Crescent 03DD004: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 88% Analysis Date = 11/06/14 SpikeMix = Spex Organics C1140417015: 10 µl & Crescent 03DD004: 10 µl Pct Recovery = 106% Analysis Date = 09/09/14 SpikeMix = NSI 032614: 10 µl & Spex Organics C1140417015: 10 µl Pct Recovery = 122% Analysis Date = 07/23/14 SpikeMix = Spex Organics C1140417015: 10 µl & Accu 214031115: 10 µl Pct Recovery = 96% Analysis Date = 07/11/14 SpikeMix = Spex Organics C1140417015: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 107% Analysis Date = 11/20/15 SpikeMix = Accu 215041380: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 98% Analysis Date = 07/31/15 SpikeMix = Crescent 04EE008: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 96% Analysis Date = 06/27/15 SpikeMix = ERA 0406-15-03: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 94% Analysis Date = 03/17/16 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 98% Analysis Date = 01/27/16 SpikeMix = Crescent 04EE008: 10 µl & NSI 050515AVOC: 10 µl Pct Recovery = 87% Analysis Date = 12/10/15 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 91% Analysis Date = 09/03/15 SpikeMix = NSI 050515AVOC: 10 µl & Spex Organics EN150428007: 10 µl Pct Recovery = 79% Analysis Date = 12/12/16 Pct Recovery = 97% Analysis Date = 12/07/16 Pct Recovery = 97% Analysis Date = 12/07/16 Pct Recovery = 97% Analysis Date = 12/02/16 Pct Recovery = 97% Analysis Date = 12/02/16 Pct Recovery = 97% Analysis Date = 11/27/16 Pct Recovery = 97% Analysis Date = 11/27/16 Pct Recovery = 97% Analysis Date = 11/22/16 Pct Recovery = 97% Analysis Date = 11/22/16 Pct Recovery = 97% Analysis Date = 11/18/16 Pct Recovery = 97% Analysis Date = 11/18/16 Pct Recovery = 97% Analysis Date = 11/13/16 Pct Recovery = 97% Analysis Date = 11/13/16 Pct Recovery = 97% Analysis Date = 11/08/16 Pct Recovery = 97% Analysis Date = 11/08/16 Pct Recovery = 97% Analysis Date = 11/03/16 Pct Recovery = 97% Analysis Date = 11/03/16 Pct Recovery = 97% Analysis Date = 10/30/16 Pct Recovery = 97% Analysis Date = 10/30/16 Pct Recovery = 97% Analysis Date = 10/25/16 Pct Recovery = 97% Analysis Date = 10/25/16 Pct Recovery = 97% Analysis Date = 10/20/16 Pct Recovery = 97% Analysis Date = 10/20/16 Pct Recovery = 97% Analysis Date = 10/15/16 Pct Recovery = 97% Analysis Date = 10/15/16 Pct Recovery = 97% Analysis Date = 10/10/16 Pct Recovery = 97% Analysis Date = 10/10/16 Pct Recovery = 97% Analysis Date = 10/06/16 Pct Recovery = 97% Analysis Date = 10/06/16 Pct Recovery = 97% Analysis Date = 10/01/16 Pct Recovery = 96% Analysis Date = 10/01/16 Pct Recovery = 96% Analysis Date = 09/26/16 Pct Recovery = 96% Analysis Date = 09/26/16 Pct Recovery = 96% Analysis Date = 09/21/16 Pct Recovery = 96% Analysis Date = 09/21/16 Pct Recovery = 96% Analysis Date = 09/17/16 Pct Recovery = 96% Analysis Date = 09/17/16 Pct Recovery = 96% Analysis Date = 09/12/16 Pct Recovery = 96% Analysis Date = 09/12/16 Pct Recovery = 96% Analysis Date = 09/07/16 Pct Recovery = 96% Analysis Date = 09/07/16 Pct Recovery = 96% Analysis Date = 09/02/16 Pct Recovery = 96% Analysis Date = 09/02/16 Pct Recovery = 96% Analysis Date = 08/29/16 Pct Recovery = 96% Analysis Date = 08/29/16 Pct Recovery = 96% Analysis Date = 08/24/16 Pct Recovery = 96% Analysis Date = 08/24/16 Pct Recovery = 96% Analysis Date = 08/19/16 Pct Recovery = 96% Analysis Date = 08/19/16 Pct Recovery = 96% Analysis Date = 08/14/16 Pct Recovery = 96% Analysis Date = 08/14/16 Pct Recovery = 96% Analysis Date = 08/09/16 Pct Recovery = 96% Analysis Date = 08/09/16 Pct Recovery = 96% Analysis Date = 08/05/16 Pct Recovery = 96% Analysis Date = 08/05/16 Pct Recovery = 96% Analysis Date = 07/31/16 Pct Recovery = 96% Analysis Date = 07/31/16 Pct Recovery = 96% Analysis Date = 07/26/16 Pct Recovery = 96% Analysis Date = 07/26/16 Pct Recovery = 96% Analysis Date = 07/21/16 Pct Recovery = 96% Analysis Date = 07/21/16 Pct Recovery = 96% Analysis Date = 07/17/16 Pct Recovery = 96% Analysis Date = 07/17/16 Pct Recovery = 96% Analysis Date = 07/12/16 Pct Recovery = 96% Analysis Date = 07/12/16 Pct Recovery = 96% Analysis Date = 07/07/16 Pct Recovery = 96% Analysis Date = 07/07/16 Pct Recovery = 96% Analysis Date = 07/02/16 Pct Recovery = 96% Analysis Date = 07/02/16 Pct Recovery = 96% Analysis Date = 06/28/16 Pct Recovery = 95% Analysis Date = 06/28/16 Pct Recovery = 95% Analysis Date = 06/23/16 Pct Recovery = 95% Analysis Date = 06/23/16 Pct Recovery = 95% Analysis Date = 06/18/16 Pct Recovery = 95% Analysis Date = 06/18/16 Pct Recovery = 95% Analysis Date = 06/13/16 Pct Recovery = 95% Analysis Date = 06/13/16 Pct Recovery = 95% Analysis Date = 06/08/16 Pct Recovery = 95% Analysis Date = 06/08/16 Pct Recovery = 95% Analysis Date = 06/04/16 Pct Recovery = 95% Analysis Date = 06/04/16 Pct Recovery = 95% Analysis Date = 05/30/16 Pct Recovery = 95% Analysis Date = 05/30/16 Pct Recovery = 95% Analysis Date = 05/25/16 Pct Recovery = 95% Analysis Date = 05/25/16 Pct Recovery = 95% Analysis Date = 05/20/16 Pct Recovery = 95% Analysis Date = 05/20/16 Pct Recovery = 95% Analysis Date = 05/16/16 Pct Recovery = 95% Analysis Date = 05/16/16 Pct Recovery = 95% Analysis Date = 05/11/16 Pct Recovery = 95% Analysis Date = 05/11/16 Pct Recovery = 95% Analysis Date = 05/06/16 Pct Recovery = 95% Analysis Date = 05/06/16 Pct Recovery = 95% Analysis Date = 05/01/16 Pct Recovery = 95% Analysis Date = 05/01/16 Pct Recovery = 95% Analysis Date = 04/27/16 Pct Recovery = 95% Analysis Date = 04/27/16 Pct Recovery = 95% Analysis Date = 04/22/16 Pct Recovery = 95% Analysis Date = 04/22/16 Pct Recovery = 95% Analysis Date = 04/17/16 Pct Recovery = 95% Analysis Date = 04/17/16 Pct Recovery = 95% Analysis Date = 04/12/16 Pct Recovery = 95% Analysis Date = 04/12/16 Pct Recovery = 95% Analysis Date = 04/07/16 Pct Recovery = 95% Analysis Date = 04/07/16 Pct Recovery = 95% Analysis Date = 04/03/16 Pct Recovery = 95% Analysis Date = 04/03/16 Pct Recovery = 95% Analysis Date = 03/29/16 Pct Recovery = 95% Analysis Date = 03/29/16 Pct Recovery = 95% Analysis Date = 03/24/16 Pct Recovery = 95% Analysis Date = 03/24/16 Pct Recovery = 95% Analysis Date = 03/19/16 Pct Recovery = 94% Analysis Date = 03/19/16 Pct Recovery = 94% Analysis Date = 03/15/16 Pct Recovery = 94% Analysis Date = 03/15/16 Pct Recovery = 94% Analysis Date = 03/10/16 Pct Recovery = 94% Analysis Date = 03/10/16 Pct Recovery = 94% Analysis Date = 03/05/16 Pct Recovery = 94% Analysis Date = 03/05/16 Pct Recovery = 94% Analysis Date = 02/29/16 Pct Recovery = 94% Analysis Date = 02/29/16 Pct Recovery = 94% Analysis Date = 02/25/16 Pct Recovery = 94% Analysis Date = 02/25/16 Pct Recovery = 94% Analysis Date = 02/20/16 Pct Recovery = 94% Analysis Date = 02/20/16 Pct Recovery = 94% Analysis Date = 02/15/16 Pct Recovery = 94% Analysis Date = 02/15/16 Pct Recovery = 94% Analysis Date = 02/10/16 Pct Recovery = 94% Analysis Date = 02/10/16 Pct Recovery = 94% Analysis Date = 02/05/16 Pct Recovery = 94% Analysis Date = 02/05/16 Pct Recovery = 94% Analysis Date = 02/01/16 Pct Recovery = 94% Analysis Date = 02/01/16 Pct Recovery = 94% Analysis Date = 01/27/16 Pct Recovery = 93% Analysis Date = 01/27/16 Pct Recovery = 93% Analysis Date = 01/22/16 Pct Recovery = 93% Analysis Date = 01/22/16 Pct Recovery = 93% Analysis Date = 01/17/16 Pct Recovery = 93% Analysis Date = 01/17/16 Pct Recovery = 93% Analysis Date = 01/13/16 Pct Recovery = 93% Analysis Date = 01/13/16 Pct Recovery = 93% Analysis Date = 01/08/16 Pct Recovery = 93% Analysis Date = 01/08/16 Pct Recovery = 93% Analysis Date = 01/03/16 Pct Recovery = 93% Analysis Date = 01/03/16 Pct Recovery = 93% Analysis Date = 12/29/15 Pct Recovery = 93% Analysis Date = 12/29/15 Pct Recovery = 93% Analysis Date = 12/25/15 Pct Recovery = 93% Analysis Date = 12/25/15 Pct Recovery = 93% Analysis Date = 12/20/15 Pct Recovery = 93% Analysis Date = 12/20/15 Pct Recovery = 93% Analysis Date = 12/15/15 Pct Recovery = 93% Analysis Date = 12/15/15 Pct Recovery = 93% Analysis Date = 12/10/15 Pct Recovery = 93% Analysis Date = 12/10/15 Pct Recovery = 93% Analysis Date = 12/05/15 Pct Recovery = 92% Analysis Date = 12/05/15 Pct Recovery = 92% Analysis Date = 12/01/15 Pct Recovery = 92% Analysis Date = 12/01/15 Pct Recovery = 92% Analysis Date = 11/26/15 Pct Recovery = 92% Analysis Date = 11/26/15 Pct Recovery = 92% Analysis Date = 11/21/15 Pct Recovery = 92% Analysis Date = 11/21/15 Pct Recovery = 92% Analysis Date = 11/16/15 Pct Recovery = 92% Analysis Date = 11/16/15 Pct Recovery = 92% Analysis Date = 11/12/15 Pct Recovery = 92% Analysis Date = 11/12/15 Pct Recovery = 92% Analysis Date = 11/07/15 Pct Recovery = 92% Analysis Date = 11/07/15 Pct Recovery = 92% Analysis Date = 11/02/15 Pct Recovery = 92% Analysis Date = 11/02/15 Pct Recovery = 92% Analysis Date = 10/28/15 Pct Recovery = 92% Analysis Date = 10/28/15 Pct Recovery = 92% Analysis Date = 10/24/15 Pct Recovery = 92% Analysis Date = 10/24/15 Pct Recovery = 92% Analysis Date = 10/19/15 Pct Recovery = 92% Analysis Date = 10/19/15 Pct Recovery = 92% Analysis Date = 10/14/15 Pct Recovery = 92% Analysis Date = 10/14/15 Pct Recovery = 92% Analysis Date = 10/09/15 Pct Recovery = 92% Analysis Date = 10/09/15 Pct Recovery = 92% Analysis Date = 10/04/15 Pct Recovery = 92% Analysis Date = 10/04/15 Pct Recovery = 92% Analysis Date = 09/30/15 Pct Recovery = 92% Analysis Date = 09/30/15 Pct Recovery = 92% Analysis Date = 09/25/15 Pct Recovery = 92% Analysis Date = 09/25/15 Pct Recovery = 92% Analysis Date = 09/20/15 Pct Recovery = 92% Analysis Date = 09/20/15 Pct Recovery = 92% Analysis Date = 09/15/15 Pct Recovery = 92% Analysis Date = 09/15/15 Pct Recovery = 92% Analysis Date = 09/11/15 Pct Recovery = 92% Analysis Date = 09/11/15 Pct Recovery = 92% Analysis Date = 09/06/15 Pct Recovery = 93% Analysis Date = 09/06/15 Pct Recovery = 93% Analysis Date = 09/01/15 Pct Recovery = 93% Analysis Date = 09/01/15 Pct Recovery = 93% Analysis Date = 08/27/15 Pct Recovery = 93% Analysis Date = 08/27/15 Pct Recovery = 93% Analysis Date = 08/23/15 Pct Recovery = 93% Analysis Date = 08/23/15 Pct Recovery = 93% Analysis Date = 08/18/15 Pct Recovery = 93% Analysis Date = 08/18/15 Pct Recovery = 93% Analysis Date = 08/13/15 Pct Recovery = 93% Analysis Date = 08/13/15 Pct Recovery = 93% Analysis Date = 08/08/15 Pct Recovery = 93% Analysis Date = 08/08/15 Pct Recovery = 93% Analysis Date = 08/03/15 Pct Recovery = 93% Analysis Date = 08/03/15 Pct Recovery = 93% Analysis Date = 07/30/15 Pct Recovery = 93% Analysis Date = 07/30/15 Pct Recovery = 93% Analysis Date = 07/25/15 Pct Recovery = 93% Analysis Date = 07/25/15 Pct Recovery = 93% Analysis Date = 07/20/15 Pct Recovery = 93% Analysis Date = 07/20/15 Pct Recovery = 93% Analysis Date = 07/15/15 Pct Recovery = 93% Analysis Date = 07/15/15 Pct Recovery = 93% Analysis Date = 07/11/15 Pct Recovery = 94% Analysis Date = 07/11/15 Pct Recovery = 94% Analysis Date = 07/06/15 Pct Recovery = 94% Analysis Date = 07/06/15 Pct Recovery = 94% Analysis Date = 07/01/15 Pct Recovery = 94% Analysis Date = 07/01/15 Pct Recovery = 94% Analysis Date = 06/26/15 Pct Recovery = 94% Analysis Date = 06/26/15 Pct Recovery = 94% Analysis Date = 06/21/15 Pct Recovery = 94% Analysis Date = 06/21/15 Pct Recovery = 94% Analysis Date = 06/17/15 Pct Recovery = 94% Analysis Date = 06/17/15 Pct Recovery = 94% Analysis Date = 06/12/15 Pct Recovery = 94% Analysis Date = 06/12/15 Pct Recovery = 94% Analysis Date = 06/07/15 Pct Recovery = 94% Analysis Date = 06/07/15 Pct Recovery = 94% Analysis Date = 06/02/15 Pct Recovery = 94% Analysis Date = 06/02/15 Pct Recovery = 94% Analysis Date = 05/29/15 Pct Recovery = 95% Analysis Date = 05/29/15 Pct Recovery = 95% Analysis Date = 05/24/15 Pct Recovery = 95% Analysis Date = 05/24/15 Pct Recovery = 95% Analysis Date = 05/19/15 Pct Recovery = 95% Analysis Date = 05/19/15 Pct Recovery = 95% Analysis Date = 05/14/15 Pct Recovery = 95% Analysis Date = 05/14/15 Pct Recovery = 95% Analysis Date = 05/10/15 Pct Recovery = 95% Analysis Date = 05/10/15 Pct Recovery = 95% Analysis Date = 05/05/15 Pct Recovery = 95% Analysis Date = 05/05/15 Pct Recovery = 95% Analysis Date = 04/30/15 Pct Recovery = 95% Analysis Date = 04/30/15 Pct Recovery = 95% Analysis Date = 04/25/15 Pct Recovery = 95% Analysis Date = 04/25/15 Pct Recovery = 95% Analysis Date = 04/20/15 Pct Recovery = 96% Analysis Date = 04/20/15 Pct Recovery = 96% Analysis Date = 04/16/15 Pct Recovery = 96% Analysis Date = 04/16/15 Pct Recovery = 96% Analysis Date = 04/11/15 Pct Recovery = 96% Analysis Date = 04/11/15 Pct Recovery = 96% Analysis Date = 04/06/15 Pct Recovery = 96% Analysis Date = 04/06/15 Pct Recovery = 96% Analysis Date = 04/01/15 Pct Recovery = 96% Analysis Date = 04/01/15 Pct Recovery = 96% Analysis Date = 03/28/15 Pct Recovery = 96% Analysis Date = 03/28/15 Pct Recovery = 96% Analysis Date = 03/23/15 Pct Recovery = 96% Analysis Date = 03/23/15 Pct Recovery = 96% Analysis Date = 03/18/15 Pct Recovery = 96% Analysis Date = 03/18/15 Pct Recovery = 96% Analysis Date = 03/13/15 Pct Recovery = 96% Analysis Date = 03/13/15 Pct Recovery = 96% Analysis Date = 03/09/15 Pct Recovery = 96% Analysis Date = 03/09/15 Pct Recovery = 96% Analysis Date = 03/04/15 Pct Recovery = 97% Analysis Date = 03/04/15 Pct Recovery = 97% Analysis Date = 02/27/15 Pct Recovery = 97% Analysis Date = 02/27/15 Pct Recovery = 97% Analysis Date = 02/22/15 Pct Recovery = 97% Analysis Date = 02/22/15 Pct Recovery = 97% Analysis Date = 02/17/15 Pct Recovery = 97% Analysis Date = 02/17/15 Pct Recovery = 97% Analysis Date = 02/13/15 Pct Recovery = 97% Analysis Date = 02/13/15 Pct Recovery = 97% Analysis Date = 02/08/15 Pct Recovery = 97% Analysis Date = 02/08/15 Pct Recovery = 97% Analysis Date = 02/03/15 Pct Recovery = 97% Analysis Date = 02/03/15 Pct Recovery = 97% Analysis Date = 01/29/15 Pct Recovery = 97% Analysis Date = 01/29/15 Pct Recovery = 97% Analysis Date = 01/25/15 Pct Recovery = 97% Analysis Date = 01/25/15 Pct Recovery = 97% Analysis Date = 01/20/15 Pct Recovery = 97% Analysis Date = 01/20/15 Pct Recovery = 97% Analysis Date = 01/15/15 Pct Recovery = 97% Analysis Date = 01/15/15 Pct Recovery = 97% Analysis Date = 01/10/15 Pct Recovery = 97% Analysis Date = 01/10/15 Pct Recovery = 97% Analysis Date = 01/06/15 Pct Recovery = 97% Analysis Date = 01/06/15 Pct Recovery = 97% Analysis Date = 01/01/15 Pct Recovery = 97% Analysis Date = 01/01/15 Pct Recovery = 97% Analysis Date = 12/27/14 Pct Recovery = 97% Analysis Date = 12/27/14 Pct Recovery = 97% Analysis Date = 12/22/14 Pct Recovery = 97% Analysis Date = 12/22/14 Pct Recovery = 97% Analysis Date = 12/17/14 Pct Recovery = 97% Analysis Date = 12/17/14 Pct Recovery = 97% Analysis Date = 12/13/14 Pct Recovery = 97% Analysis Date = 12/13/14 Pct Recovery = 97% Analysis Date = 12/08/14 Pct Recovery = 97% Analysis Date = 12/08/14 Pct Recovery = 97% Analysis Date = 12/03/14 Pct Recovery = 97% Analysis Date = 12/03/14 Pct Recovery = 97% Analysis Date = 11/28/14 Pct Recovery = 98% Analysis Date = 11/28/14 Pct Recovery = 98% Analysis Date = 11/24/14 Pct Recovery = 98% Analysis Date = 11/24/14 Pct Recovery = 98% Analysis Date = 11/19/14 Pct Recovery = 98% Analysis Date = 11/19/14 Pct Recovery = 98% Analysis Date = 11/14/14 Pct Recovery = 98% Analysis Date = 11/14/14 Pct Recovery = 98% Analysis Date = 11/09/14 Pct Recovery = 98% Analysis Date = 11/09/14 Pct Recovery = 98% Analysis Date = 11/05/14 Pct Recovery = 98% Analysis Date = 11/05/14 Pct Recovery = 98% Analysis Date = 10/31/14 Pct Recovery = 98% Analysis Date = 10/31/14 Pct Recovery = 98% Analysis Date = 10/26/14 Pct Recovery = 98% Analysis Date = 10/26/14 Pct Recovery = 98% Analysis Date = 10/21/14 Pct Recovery = 98% Analysis Date = 10/21/14 Pct Recovery = 98% Analysis Date = 10/16/14 Pct Recovery = 98% Analysis Date = 10/16/14 Pct Recovery = 98% Analysis Date = 10/12/14 Pct Recovery = 98% Analysis Date = 10/12/14 Pct Recovery = 98% Analysis Date = 10/07/14 Pct Recovery = 98% Analysis Date = 10/07/14 Pct Recovery = 98% Analysis Date = 10/02/14 Pct Recovery = 98% Analysis Date = 10/02/14 Pct Recovery = 98% Analysis Date = 09/27/14 Pct Recovery = 98% Analysis Date = 09/27/14 Pct Recovery = 98% Analysis Date = 09/23/14 Pct Recovery = 97% Analysis Date = 09/23/14 Pct Recovery = 97% Analysis Date = 09/18/14 Pct Recovery = 97% Analysis Date = 09/18/14 Pct Recovery = 97% Analysis Date = 09/13/14 Pct Recovery = 97% Analysis Date = 09/13/14 Pct Recovery = 97% Analysis Date = 09/08/14 Pct Recovery = 97% Analysis Date = 09/08/14 Pct Recovery = 97% Analysis Date = 09/04/14 Pct Recovery = 97% Analysis Date = 09/04/14 Pct Recovery = 97% Analysis Date = 08/30/14 Pct Recovery = 97% Analysis Date = 08/30/14 Pct Recovery = 97% Analysis Date = 08/25/14 Pct Recovery = 97% Analysis Date = 08/25/14 Pct Recovery = 97% Analysis Date = 08/20/14 Pct Recovery = 97% Analysis Date = 08/20/14 Pct Recovery = 97% Analysis Date = 08/15/14 Pct Recovery = 97% Analysis Date = 08/15/14 Pct Recovery = 97% Analysis Date = 08/11/14 Pct Recovery = 97% Analysis Date = 08/11/14 Pct Recovery = 97% Analysis Date = 08/06/14 Pct Recovery = 97% Analysis Date = 08/06/14 Pct Recovery = 97% Analysis Date = 08/01/14 Pct Recovery = 97% Analysis Date = 08/01/14 Pct Recovery = 97% Analysis Date = 07/27/14 Pct Recovery = 97% Analysis Date = 07/27/14 Pct Recovery = 97% Analysis Date = 07/23/14 Pct Recovery = 96% Analysis Date = 07/23/14 Pct Recovery = 96% Analysis Date = 07/18/14 Pct Recovery = 96% Analysis Date = 07/18/14 Pct Recovery = 96% Analysis Date = 07/13/14 Pct Recovery = 96% Analysis Date = 07/13/14 Pct Recovery = 96% Analysis Date = 07/08/14 Pct Recovery = 96% Analysis Date = 07/08/14 Pct Recovery = 96% Analysis Date = 07/04/14 Pct Recovery = 96% Analysis Date = 07/04/14 Pct Recovery = 96% Analysis Date = 06/29/14 Pct Recovery = 96% Analysis Date = 06/29/14 Pct Recovery = 96% Analysis Date = 06/24/14 Pct Recovery = 96% Analysis Date = 06/24/14 Pct Recovery = 96% Analysis Date = 06/19/14 Pct Recovery = 96% Analysis Date = 06/19/14 Pct Recovery = 96% Analysis Date = 06/14/14 Pct Recovery = 96% Analysis Date = 06/14/14 Pct Recovery = 96% Analysis Date = 06/10/14 Pct Recovery = 95% Analysis Date = 06/10/14 Pct Recovery = 95% Analysis Date = 06/05/14 Pct Recovery = 95% Analysis Date = 06/05/14 Pct Recovery = 95% Analysis Date = 05/31/14 Pct Recovery = 95% Analysis Date = 05/31/14 Pct Recovery = 95% Analysis Date = 05/26/14 Pct Recovery = 95% Analysis Date = 05/26/14 Pct Recovery = 95% Analysis Date = 05/22/14 Pct Recovery = 95% Analysis Date = 05/22/14 Pct Recovery = 95% Analysis Date = 05/17/14 Pct Recovery = 95% Analysis Date = 05/17/14 Pct Recovery = 95% Analysis Date = 05/12/14 Pct Recovery = 95% Analysis Date = 05/12/14 Pct Recovery = 95% Analysis Date = 05/07/14 Pct Recovery = 95% Analysis Date = 05/07/14 Pct Recovery = 95% Analysis Date = 05/03/14 Pct Recovery = 94% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
1,2-DICHLOROBENZENE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 42 95% 10% 96% 11%
Total 42 95% 10% 96% 11%

Sample Statistics
1,2-DICHLOROBENZENE

Characteristic N % % Basis
Plotted 42 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 42 .  
False Negatives 0 0% 0 out of 42
Not Spiked 24 .  
False Positives 0 0% 0 out of 24

BQS OBSP Determination:
1,2-DICHLOROETHANE
METHOD: 4440 , TESTIDCODE: 32103GCM66
Open Data Set

Analysis Date = 12/12/16 SpikeMix = Accu 216041125: 40 µl & Crescent 03FF058: 40 µl Pct Recovery = 96% Analysis Date = 07/20/16 SpikeMix = Supelco LC20141V: 40 µl & Accu 216041125: 40 µl Pct Recovery = 97% Analysis Date = 08/12/16 SpikeMix = ChemService 5082900: 25 µl & Phenova B20160319: 25 µl Pct Recovery = 96% Analysis Date = 06/21/16 SpikeMix = Phenova B20160319: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 101% Analysis Date = 09/08/16 SpikeMix = Supelco LC20141V: 25 µl & Accu 216041125: 25 µl Pct Recovery = 87% Analysis Date = 05/24/16 SpikeMix = Accu 216041125: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 94% Analysis Date = 04/09/15 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 106% Analysis Date = 03/06/15 SpikeMix = ERA 0227-14-06.1A: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 98% Analysis Date = 11/14/14 SpikeMix = Crescent 03DD004: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 93% Analysis Date = 08/16/14 SpikeMix = ERA 0227-14-06.1A: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 105% Analysis Date = 07/01/14 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 110% Analysis Date = 11/22/14 SpikeMix = NSI 032614: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 106% Analysis Date = 06/10/14 SpikeMix = Crescent 03DD004: 20 µl & NSI 032614: 20 µl Pct Recovery = 103% Analysis Date = 06/10/14 SpikeMix = NSI 032614: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 102% Analysis Date = 05/01/14 SpikeMix = Accu 214031115: 20 µl & NSI 032614: 20 µl Pct Recovery = 105% Analysis Date = 07/13/15 SpikeMix = Crescent 04EE008: 25 µl & NSI 050515AVOC: 25 µl Pct Recovery = 99% Analysis Date = 09/29/15 SpikeMix = Accu 215041380: 25 µl & ERA 0406-15-03: 25 µl Pct Recovery = 97% Analysis Date = 06/16/15 SpikeMix = ERA 0406-15-03: 25 µl & Supelco LC13545: 25 µl Pct Recovery = 92% Analysis Date = 11/29/16 SpikeMix = ChemService 5082900: 15 µl & Phenova B20160319: 15 µl Pct Recovery = 94% Analysis Date = 09/08/16 SpikeMix = Phenova B20160319: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 99% Analysis Date = 05/27/16 SpikeMix = Phenova B20160319: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 96% Analysis Date = 08/20/16 SpikeMix = Accu 216041125: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 95% Analysis Date = 06/30/16 SpikeMix = ChemService 5082900: 15 µl & Accu 216041125: 15 µl Pct Recovery = 68% Analysis Date = 11/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 90% Analysis Date = 10/17/15 SpikeMix = Crescent 04EE008: 15 µl & NSI 050515AVOC: 15 µl Pct Recovery = 89% Analysis Date = 06/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Accu 215041380: 15 µl Pct Recovery = 97% Analysis Date = 04/26/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 96% Analysis Date = 03/04/16 SpikeMix = Accu 215041380: 15 µl & ERA 0406-15-03: 15 µl Pct Recovery = 95% Analysis Date = 02/05/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 95% Analysis Date = 10/16/15 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 92% Analysis Date = 01/13/15 SpikeMix = Accu 214031115: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 103% Analysis Date = 10/21/14 SpikeMix = ERA 0227-14-06.1A: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 92% Analysis Date = 10/04/14 SpikeMix = Crescent 03DD004: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 103% Analysis Date = 07/11/14 SpikeMix = Spex Organics C1140417015: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 106% Analysis Date = 09/09/14 SpikeMix = Accu 214031115: 10 µl & NSI 032614: 10 µl Pct Recovery = 107% Analysis Date = 09/09/14 SpikeMix = NSI 032614: 10 µl & Spex Organics C1140417015: 10 µl Pct Recovery = 108% Analysis Date = 07/29/14 SpikeMix = Crescent 03DD004: 10 µl & NSI 032614: 10 µl Pct Recovery = 103% Analysis Date = 05/30/14 SpikeMix = NSI 032614: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 92% Analysis Date = 03/17/16 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 93% Analysis Date = 01/27/16 SpikeMix = Crescent 04EE008: 10 µl & NSI 050515AVOC: 10 µl Pct Recovery = 97% Analysis Date = 12/10/15 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 97% Analysis Date = 09/03/15 SpikeMix = NSI 050515AVOC: 10 µl & Spex Organics EN150428007: 10 µl Pct Recovery = 87% Analysis Date = 11/20/15 SpikeMix = Accu 215041380: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 97% Analysis Date = 07/31/15 SpikeMix = Crescent 04EE008: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 95% Analysis Date = 06/27/15 SpikeMix = ERA 0406-15-03: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 104% Analysis Date = 12/11/16 Pct Recovery = 94% Analysis Date = 12/07/16 Pct Recovery = 94% Analysis Date = 12/07/16 Pct Recovery = 94% Analysis Date = 12/02/16 Pct Recovery = 94% Analysis Date = 12/02/16 Pct Recovery = 94% Analysis Date = 11/27/16 Pct Recovery = 94% Analysis Date = 11/27/16 Pct Recovery = 94% Analysis Date = 11/22/16 Pct Recovery = 94% Analysis Date = 11/22/16 Pct Recovery = 94% Analysis Date = 11/18/16 Pct Recovery = 94% Analysis Date = 11/18/16 Pct Recovery = 94% Analysis Date = 11/13/16 Pct Recovery = 94% Analysis Date = 11/13/16 Pct Recovery = 94% Analysis Date = 11/08/16 Pct Recovery = 94% Analysis Date = 11/08/16 Pct Recovery = 94% Analysis Date = 11/03/16 Pct Recovery = 94% Analysis Date = 11/03/16 Pct Recovery = 94% Analysis Date = 10/29/16 Pct Recovery = 94% Analysis Date = 10/29/16 Pct Recovery = 94% Analysis Date = 10/25/16 Pct Recovery = 94% Analysis Date = 10/25/16 Pct Recovery = 94% Analysis Date = 10/20/16 Pct Recovery = 94% Analysis Date = 10/20/16 Pct Recovery = 94% Analysis Date = 10/15/16 Pct Recovery = 94% Analysis Date = 10/15/16 Pct Recovery = 94% Analysis Date = 10/10/16 Pct Recovery = 94% Analysis Date = 10/10/16 Pct Recovery = 94% Analysis Date = 10/06/16 Pct Recovery = 94% Analysis Date = 10/06/16 Pct Recovery = 94% Analysis Date = 10/01/16 Pct Recovery = 94% Analysis Date = 10/01/16 Pct Recovery = 94% Analysis Date = 09/26/16 Pct Recovery = 94% Analysis Date = 09/26/16 Pct Recovery = 94% Analysis Date = 09/21/16 Pct Recovery = 94% Analysis Date = 09/21/16 Pct Recovery = 94% Analysis Date = 09/16/16 Pct Recovery = 94% Analysis Date = 09/16/16 Pct Recovery = 94% Analysis Date = 09/12/16 Pct Recovery = 94% Analysis Date = 09/12/16 Pct Recovery = 94% Analysis Date = 09/07/16 Pct Recovery = 94% Analysis Date = 09/07/16 Pct Recovery = 94% Analysis Date = 09/02/16 Pct Recovery = 94% Analysis Date = 09/02/16 Pct Recovery = 94% Analysis Date = 08/28/16 Pct Recovery = 94% Analysis Date = 08/28/16 Pct Recovery = 94% Analysis Date = 08/24/16 Pct Recovery = 94% Analysis Date = 08/24/16 Pct Recovery = 94% Analysis Date = 08/19/16 Pct Recovery = 94% Analysis Date = 08/19/16 Pct Recovery = 94% Analysis Date = 08/14/16 Pct Recovery = 94% Analysis Date = 08/14/16 Pct Recovery = 94% Analysis Date = 08/09/16 Pct Recovery = 94% Analysis Date = 08/09/16 Pct Recovery = 94% Analysis Date = 08/04/16 Pct Recovery = 94% Analysis Date = 08/04/16 Pct Recovery = 94% Analysis Date = 07/31/16 Pct Recovery = 94% Analysis Date = 07/31/16 Pct Recovery = 94% Analysis Date = 07/26/16 Pct Recovery = 94% Analysis Date = 07/26/16 Pct Recovery = 94% Analysis Date = 07/21/16 Pct Recovery = 94% Analysis Date = 07/21/16 Pct Recovery = 94% Analysis Date = 07/16/16 Pct Recovery = 94% Analysis Date = 07/16/16 Pct Recovery = 94% Analysis Date = 07/12/16 Pct Recovery = 94% Analysis Date = 07/12/16 Pct Recovery = 94% Analysis Date = 07/07/16 Pct Recovery = 94% Analysis Date = 07/07/16 Pct Recovery = 94% Analysis Date = 07/02/16 Pct Recovery = 94% Analysis Date = 07/02/16 Pct Recovery = 94% Analysis Date = 06/27/16 Pct Recovery = 94% Analysis Date = 06/27/16 Pct Recovery = 94% Analysis Date = 06/22/16 Pct Recovery = 94% Analysis Date = 06/22/16 Pct Recovery = 94% Analysis Date = 06/18/16 Pct Recovery = 94% Analysis Date = 06/18/16 Pct Recovery = 94% Analysis Date = 06/13/16 Pct Recovery = 94% Analysis Date = 06/13/16 Pct Recovery = 94% Analysis Date = 06/08/16 Pct Recovery = 94% Analysis Date = 06/08/16 Pct Recovery = 94% Analysis Date = 06/03/16 Pct Recovery = 94% Analysis Date = 06/03/16 Pct Recovery = 94% Analysis Date = 05/30/16 Pct Recovery = 94% Analysis Date = 05/30/16 Pct Recovery = 94% Analysis Date = 05/25/16 Pct Recovery = 94% Analysis Date = 05/25/16 Pct Recovery = 94% Analysis Date = 05/20/16 Pct Recovery = 94% Analysis Date = 05/20/16 Pct Recovery = 94% Analysis Date = 05/15/16 Pct Recovery = 94% Analysis Date = 05/15/16 Pct Recovery = 94% Analysis Date = 05/10/16 Pct Recovery = 94% Analysis Date = 05/10/16 Pct Recovery = 94% Analysis Date = 05/06/16 Pct Recovery = 94% Analysis Date = 05/06/16 Pct Recovery = 94% Analysis Date = 05/01/16 Pct Recovery = 94% Analysis Date = 05/01/16 Pct Recovery = 94% Analysis Date = 04/26/16 Pct Recovery = 94% Analysis Date = 04/26/16 Pct Recovery = 94% Analysis Date = 04/21/16 Pct Recovery = 94% Analysis Date = 04/21/16 Pct Recovery = 94% Analysis Date = 04/16/16 Pct Recovery = 94% Analysis Date = 04/16/16 Pct Recovery = 94% Analysis Date = 04/12/16 Pct Recovery = 94% Analysis Date = 04/12/16 Pct Recovery = 94% Analysis Date = 04/07/16 Pct Recovery = 94% Analysis Date = 04/07/16 Pct Recovery = 94% Analysis Date = 04/02/16 Pct Recovery = 94% Analysis Date = 04/02/16 Pct Recovery = 94% Analysis Date = 03/28/16 Pct Recovery = 94% Analysis Date = 03/28/16 Pct Recovery = 94% Analysis Date = 03/24/16 Pct Recovery = 94% Analysis Date = 03/24/16 Pct Recovery = 94% Analysis Date = 03/19/16 Pct Recovery = 94% Analysis Date = 03/19/16 Pct Recovery = 94% Analysis Date = 03/14/16 Pct Recovery = 94% Analysis Date = 03/14/16 Pct Recovery = 94% Analysis Date = 03/09/16 Pct Recovery = 94% Analysis Date = 03/09/16 Pct Recovery = 94% Analysis Date = 03/04/16 Pct Recovery = 94% Analysis Date = 03/04/16 Pct Recovery = 94% Analysis Date = 02/29/16 Pct Recovery = 94% Analysis Date = 02/29/16 Pct Recovery = 94% Analysis Date = 02/24/16 Pct Recovery = 94% Analysis Date = 02/24/16 Pct Recovery = 94% Analysis Date = 02/19/16 Pct Recovery = 94% Analysis Date = 02/19/16 Pct Recovery = 94% Analysis Date = 02/14/16 Pct Recovery = 94% Analysis Date = 02/14/16 Pct Recovery = 94% Analysis Date = 02/10/16 Pct Recovery = 94% Analysis Date = 02/10/16 Pct Recovery = 94% Analysis Date = 02/05/16 Pct Recovery = 94% Analysis Date = 02/05/16 Pct Recovery = 94% Analysis Date = 01/31/16 Pct Recovery = 94% Analysis Date = 01/31/16 Pct Recovery = 94% Analysis Date = 01/26/16 Pct Recovery = 94% Analysis Date = 01/26/16 Pct Recovery = 94% Analysis Date = 01/21/16 Pct Recovery = 94% Analysis Date = 01/21/16 Pct Recovery = 94% Analysis Date = 01/17/16 Pct Recovery = 94% Analysis Date = 01/17/16 Pct Recovery = 94% Analysis Date = 01/12/16 Pct Recovery = 94% Analysis Date = 01/12/16 Pct Recovery = 94% Analysis Date = 01/07/16 Pct Recovery = 94% Analysis Date = 01/07/16 Pct Recovery = 94% Analysis Date = 01/02/16 Pct Recovery = 94% Analysis Date = 01/02/16 Pct Recovery = 94% Analysis Date = 12/29/15 Pct Recovery = 94% Analysis Date = 12/29/15 Pct Recovery = 94% Analysis Date = 12/24/15 Pct Recovery = 94% Analysis Date = 12/24/15 Pct Recovery = 94% Analysis Date = 12/19/15 Pct Recovery = 94% Analysis Date = 12/19/15 Pct Recovery = 94% Analysis Date = 12/14/15 Pct Recovery = 94% Analysis Date = 12/14/15 Pct Recovery = 94% Analysis Date = 12/09/15 Pct Recovery = 94% Analysis Date = 12/09/15 Pct Recovery = 94% Analysis Date = 12/05/15 Pct Recovery = 94% Analysis Date = 12/05/15 Pct Recovery = 94% Analysis Date = 11/30/15 Pct Recovery = 94% Analysis Date = 11/30/15 Pct Recovery = 94% Analysis Date = 11/25/15 Pct Recovery = 94% Analysis Date = 11/25/15 Pct Recovery = 94% Analysis Date = 11/20/15 Pct Recovery = 95% Analysis Date = 11/20/15 Pct Recovery = 95% Analysis Date = 11/16/15 Pct Recovery = 95% Analysis Date = 11/16/15 Pct Recovery = 95% Analysis Date = 11/11/15 Pct Recovery = 95% Analysis Date = 11/11/15 Pct Recovery = 95% Analysis Date = 11/06/15 Pct Recovery = 95% Analysis Date = 11/06/15 Pct Recovery = 95% Analysis Date = 11/01/15 Pct Recovery = 95% Analysis Date = 11/01/15 Pct Recovery = 95% Analysis Date = 10/27/15 Pct Recovery = 95% Analysis Date = 10/27/15 Pct Recovery = 95% Analysis Date = 10/23/15 Pct Recovery = 95% Analysis Date = 10/23/15 Pct Recovery = 95% Analysis Date = 10/18/15 Pct Recovery = 95% Analysis Date = 10/18/15 Pct Recovery = 95% Analysis Date = 10/13/15 Pct Recovery = 95% Analysis Date = 10/13/15 Pct Recovery = 95% Analysis Date = 10/08/15 Pct Recovery = 95% Analysis Date = 10/08/15 Pct Recovery = 95% Analysis Date = 10/04/15 Pct Recovery = 95% Analysis Date = 10/04/15 Pct Recovery = 95% Analysis Date = 09/29/15 Pct Recovery = 95% Analysis Date = 09/29/15 Pct Recovery = 95% Analysis Date = 09/24/15 Pct Recovery = 95% Analysis Date = 09/24/15 Pct Recovery = 95% Analysis Date = 09/19/15 Pct Recovery = 96% Analysis Date = 09/19/15 Pct Recovery = 96% Analysis Date = 09/14/15 Pct Recovery = 96% Analysis Date = 09/14/15 Pct Recovery = 96% Analysis Date = 09/10/15 Pct Recovery = 96% Analysis Date = 09/10/15 Pct Recovery = 96% Analysis Date = 09/05/15 Pct Recovery = 96% Analysis Date = 09/05/15 Pct Recovery = 96% Analysis Date = 08/31/15 Pct Recovery = 96% Analysis Date = 08/31/15 Pct Recovery = 96% Analysis Date = 08/26/15 Pct Recovery = 96% Analysis Date = 08/26/15 Pct Recovery = 96% Analysis Date = 08/21/15 Pct Recovery = 96% Analysis Date = 08/21/15 Pct Recovery = 96% Analysis Date = 08/17/15 Pct Recovery = 96% Analysis Date = 08/17/15 Pct Recovery = 96% Analysis Date = 08/12/15 Pct Recovery = 96% Analysis Date = 08/12/15 Pct Recovery = 96% Analysis Date = 08/07/15 Pct Recovery = 96% Analysis Date = 08/07/15 Pct Recovery = 96% Analysis Date = 08/02/15 Pct Recovery = 96% Analysis Date = 08/02/15 Pct Recovery = 96% Analysis Date = 07/29/15 Pct Recovery = 96% Analysis Date = 07/29/15 Pct Recovery = 96% Analysis Date = 07/24/15 Pct Recovery = 96% Analysis Date = 07/24/15 Pct Recovery = 96% Analysis Date = 07/19/15 Pct Recovery = 97% Analysis Date = 07/19/15 Pct Recovery = 97% Analysis Date = 07/14/15 Pct Recovery = 97% Analysis Date = 07/14/15 Pct Recovery = 97% Analysis Date = 07/09/15 Pct Recovery = 97% Analysis Date = 07/09/15 Pct Recovery = 97% Analysis Date = 07/05/15 Pct Recovery = 97% Analysis Date = 07/05/15 Pct Recovery = 97% Analysis Date = 06/30/15 Pct Recovery = 97% Analysis Date = 06/30/15 Pct Recovery = 97% Analysis Date = 06/25/15 Pct Recovery = 97% Analysis Date = 06/25/15 Pct Recovery = 97% Analysis Date = 06/20/15 Pct Recovery = 97% Analysis Date = 06/20/15 Pct Recovery = 97% Analysis Date = 06/16/15 Pct Recovery = 97% Analysis Date = 06/16/15 Pct Recovery = 97% Analysis Date = 06/11/15 Pct Recovery = 97% Analysis Date = 06/11/15 Pct Recovery = 97% Analysis Date = 06/06/15 Pct Recovery = 97% Analysis Date = 06/06/15 Pct Recovery = 97% Analysis Date = 06/01/15 Pct Recovery = 97% Analysis Date = 06/01/15 Pct Recovery = 97% Analysis Date = 05/27/15 Pct Recovery = 98% Analysis Date = 05/27/15 Pct Recovery = 98% Analysis Date = 05/23/15 Pct Recovery = 98% Analysis Date = 05/23/15 Pct Recovery = 98% Analysis Date = 05/18/15 Pct Recovery = 98% Analysis Date = 05/18/15 Pct Recovery = 98% Analysis Date = 05/13/15 Pct Recovery = 98% Analysis Date = 05/13/15 Pct Recovery = 98% Analysis Date = 05/08/15 Pct Recovery = 98% Analysis Date = 05/08/15 Pct Recovery = 98% Analysis Date = 05/04/15 Pct Recovery = 98% Analysis Date = 05/04/15 Pct Recovery = 98% Analysis Date = 04/29/15 Pct Recovery = 98% Analysis Date = 04/29/15 Pct Recovery = 98% Analysis Date = 04/24/15 Pct Recovery = 98% Analysis Date = 04/24/15 Pct Recovery = 98% Analysis Date = 04/19/15 Pct Recovery = 98% Analysis Date = 04/19/15 Pct Recovery = 98% Analysis Date = 04/14/15 Pct Recovery = 99% Analysis Date = 04/14/15 Pct Recovery = 99% Analysis Date = 04/10/15 Pct Recovery = 99% Analysis Date = 04/10/15 Pct Recovery = 99% Analysis Date = 04/05/15 Pct Recovery = 99% Analysis Date = 04/05/15 Pct Recovery = 99% Analysis Date = 03/31/15 Pct Recovery = 99% Analysis Date = 03/31/15 Pct Recovery = 99% Analysis Date = 03/26/15 Pct Recovery = 99% Analysis Date = 03/26/15 Pct Recovery = 99% Analysis Date = 03/22/15 Pct Recovery = 99% Analysis Date = 03/22/15 Pct Recovery = 99% Analysis Date = 03/17/15 Pct Recovery = 99% Analysis Date = 03/17/15 Pct Recovery = 99% Analysis Date = 03/12/15 Pct Recovery = 99% Analysis Date = 03/12/15 Pct Recovery = 99% Analysis Date = 03/07/15 Pct Recovery = 99% Analysis Date = 03/07/15 Pct Recovery = 99% Analysis Date = 03/02/15 Pct Recovery = 100% Analysis Date = 03/02/15 Pct Recovery = 100% Analysis Date = 02/26/15 Pct Recovery = 100% Analysis Date = 02/26/15 Pct Recovery = 100% Analysis Date = 02/21/15 Pct Recovery = 100% Analysis Date = 02/21/15 Pct Recovery = 100% Analysis Date = 02/16/15 Pct Recovery = 100% Analysis Date = 02/16/15 Pct Recovery = 100% Analysis Date = 02/11/15 Pct Recovery = 100% Analysis Date = 02/11/15 Pct Recovery = 100% Analysis Date = 02/07/15 Pct Recovery = 100% Analysis Date = 02/07/15 Pct Recovery = 100% Analysis Date = 02/02/15 Pct Recovery = 100% Analysis Date = 02/02/15 Pct Recovery = 100% Analysis Date = 01/28/15 Pct Recovery = 100% Analysis Date = 01/28/15 Pct Recovery = 100% Analysis Date = 01/23/15 Pct Recovery = 100% Analysis Date = 01/23/15 Pct Recovery = 100% Analysis Date = 01/18/15 Pct Recovery = 101% Analysis Date = 01/18/15 Pct Recovery = 101% Analysis Date = 01/14/15 Pct Recovery = 101% Analysis Date = 01/14/15 Pct Recovery = 101% Analysis Date = 01/09/15 Pct Recovery = 101% Analysis Date = 01/09/15 Pct Recovery = 101% Analysis Date = 01/04/15 Pct Recovery = 101% Analysis Date = 01/04/15 Pct Recovery = 101% Analysis Date = 12/30/14 Pct Recovery = 101% Analysis Date = 12/30/14 Pct Recovery = 101% Analysis Date = 12/25/14 Pct Recovery = 101% Analysis Date = 12/25/14 Pct Recovery = 101% Analysis Date = 12/21/14 Pct Recovery = 101% Analysis Date = 12/21/14 Pct Recovery = 101% Analysis Date = 12/16/14 Pct Recovery = 101% Analysis Date = 12/16/14 Pct Recovery = 101% Analysis Date = 12/11/14 Pct Recovery = 101% Analysis Date = 12/11/14 Pct Recovery = 101% Analysis Date = 12/06/14 Pct Recovery = 101% Analysis Date = 12/06/14 Pct Recovery = 101% Analysis Date = 12/02/14 Pct Recovery = 101% Analysis Date = 12/02/14 Pct Recovery = 101% Analysis Date = 11/27/14 Pct Recovery = 101% Analysis Date = 11/27/14 Pct Recovery = 101% Analysis Date = 11/22/14 Pct Recovery = 101% Analysis Date = 11/22/14 Pct Recovery = 101% Analysis Date = 11/17/14 Pct Recovery = 101% Analysis Date = 11/17/14 Pct Recovery = 101% Analysis Date = 11/12/14 Pct Recovery = 101% Analysis Date = 11/12/14 Pct Recovery = 101% Analysis Date = 11/08/14 Pct Recovery = 102% Analysis Date = 11/08/14 Pct Recovery = 102% Analysis Date = 11/03/14 Pct Recovery = 102% Analysis Date = 11/03/14 Pct Recovery = 102% Analysis Date = 10/29/14 Pct Recovery = 102% Analysis Date = 10/29/14 Pct Recovery = 102% Analysis Date = 10/24/14 Pct Recovery = 102% Analysis Date = 10/24/14 Pct Recovery = 102% Analysis Date = 10/20/14 Pct Recovery = 102% Analysis Date = 10/20/14 Pct Recovery = 102% Analysis Date = 10/15/14 Pct Recovery = 102% Analysis Date = 10/15/14 Pct Recovery = 102% Analysis Date = 10/10/14 Pct Recovery = 102% Analysis Date = 10/10/14 Pct Recovery = 102% Analysis Date = 10/05/14 Pct Recovery = 102% Analysis Date = 10/05/14 Pct Recovery = 102% Analysis Date = 09/30/14 Pct Recovery = 102% Analysis Date = 09/30/14 Pct Recovery = 102% Analysis Date = 09/26/14 Pct Recovery = 102% Analysis Date = 09/26/14 Pct Recovery = 102% Analysis Date = 09/21/14 Pct Recovery = 102% Analysis Date = 09/21/14 Pct Recovery = 102% Analysis Date = 09/16/14 Pct Recovery = 102% Analysis Date = 09/16/14 Pct Recovery = 102% Analysis Date = 09/11/14 Pct Recovery = 102% Analysis Date = 09/11/14 Pct Recovery = 102% Analysis Date = 09/07/14 Pct Recovery = 102% Analysis Date = 09/07/14 Pct Recovery = 102% Analysis Date = 09/02/14 Pct Recovery = 102% Analysis Date = 09/02/14 Pct Recovery = 102% Analysis Date = 08/28/14 Pct Recovery = 102% Analysis Date = 08/28/14 Pct Recovery = 102% Analysis Date = 08/23/14 Pct Recovery = 102% Analysis Date = 08/23/14 Pct Recovery = 102% Analysis Date = 08/18/14 Pct Recovery = 102% Analysis Date = 08/18/14 Pct Recovery = 102% Analysis Date = 08/14/14 Pct Recovery = 102% Analysis Date = 08/14/14 Pct Recovery = 102% Analysis Date = 08/09/14 Pct Recovery = 103% Analysis Date = 08/09/14 Pct Recovery = 103% Analysis Date = 08/04/14 Pct Recovery = 103% Analysis Date = 08/04/14 Pct Recovery = 103% Analysis Date = 07/30/14 Pct Recovery = 103% Analysis Date = 07/30/14 Pct Recovery = 103% Analysis Date = 07/26/14 Pct Recovery = 103% Analysis Date = 07/26/14 Pct Recovery = 103% Analysis Date = 07/21/14 Pct Recovery = 103% Analysis Date = 07/21/14 Pct Recovery = 103% Analysis Date = 07/16/14 Pct Recovery = 103% Analysis Date = 07/16/14 Pct Recovery = 103% Analysis Date = 07/11/14 Pct Recovery = 103% Analysis Date = 07/11/14 Pct Recovery = 103% Analysis Date = 07/06/14 Pct Recovery = 103% Analysis Date = 07/06/14 Pct Recovery = 103% Analysis Date = 07/02/14 Pct Recovery = 103% Analysis Date = 07/02/14 Pct Recovery = 103% Analysis Date = 06/27/14 Pct Recovery = 103% Analysis Date = 06/27/14 Pct Recovery = 103% Analysis Date = 06/22/14 Pct Recovery = 103% Analysis Date = 06/22/14 Pct Recovery = 103% Analysis Date = 06/17/14 Pct Recovery = 103% Analysis Date = 06/17/14 Pct Recovery = 103% Analysis Date = 06/13/14 Pct Recovery = 103% Analysis Date = 06/13/14 Pct Recovery = 103% Analysis Date = 06/08/14 Pct Recovery = 103% Analysis Date = 06/08/14 Pct Recovery = 103% Analysis Date = 06/03/14 Pct Recovery = 103% Analysis Date = 06/03/14 Pct Recovery = 103% Analysis Date = 05/29/14 Pct Recovery = 103% Analysis Date = 05/29/14 Pct Recovery = 103% Analysis Date = 05/24/14 Pct Recovery = 103% Analysis Date = 05/24/14 Pct Recovery = 103% Analysis Date = 05/20/14 Pct Recovery = 103% Analysis Date = 05/20/14 Pct Recovery = 103% Analysis Date = 05/15/14 Pct Recovery = 103% Analysis Date = 05/15/14 Pct Recovery = 103% Analysis Date = 05/10/14 Pct Recovery = 103% Analysis Date = 05/10/14 Pct Recovery = 103% Analysis Date = 05/05/14 Pct Recovery = 104% Analysis Date = 05/05/14 Pct Recovery = 104% Analysis Date = 05/01/14 Pct Recovery = 104% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
1,2-DICHLOROETHANE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 45 97% 7% 97% 6%
Total 45 97% 7% 97% 6%

Sample Statistics
1,2-DICHLOROETHANE

Characteristic N % % Basis
Plotted 45 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 45 .  
False Negatives 0 0% 0 out of 45
Not Spiked 21 .  
False Positives 0 0% 0 out of 21

BQS OBSP Determination:
1,2-DICHLOROPROPANE
METHOD: 4440 , TESTIDCODE: 34541GCM66
Open Data Set

Analysis Date = 08/04/16 SpikeMix = Crescent 03FF058: 40 µl & Supelco LC20141V: 40 µl Pct Recovery = 83% Analysis Date = 07/20/16 SpikeMix = Supelco LC20141V: 40 µl & Accu 216041125: 40 µl Pct Recovery = 89% Analysis Date = 12/16/16 SpikeMix = NSI 041816AVOC: 40 µl & ChemService 5082900: 40 µl Pct Recovery = 127% Analysis Date = 04/09/15 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 105% Analysis Date = 08/19/14 SpikeMix = Spex Organics C1140417015: 20 µl & Accu 214031115: 20 µl Pct Recovery = 99% Analysis Date = 07/01/14 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 96% Analysis Date = 05/01/14 SpikeMix = Accu 214031115: 20 µl & NSI 032614: 20 µl Pct Recovery = 91% Analysis Date = 11/21/16 SpikeMix = Crescent 03FF058: 25 µl & Supelco LC20141V: 25 µl Pct Recovery = 89% Analysis Date = 09/08/16 SpikeMix = Supelco LC20141V: 25 µl & Accu 216041125: 25 µl Pct Recovery = 87% Analysis Date = 08/26/16 SpikeMix = NSI 041816AVOC: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 118% Analysis Date = 08/12/16 SpikeMix = ChemService 5082900: 25 µl & Phenova B20160319: 25 µl Pct Recovery = 111% Analysis Date = 06/30/16 SpikeMix = Crescent 03FF058: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 97% Analysis Date = 03/19/15 SpikeMix = Spex Organics C1140417015: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 110% Analysis Date = 12/17/14 SpikeMix = Supelco LC06438: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 97% Analysis Date = 11/14/14 SpikeMix = Crescent 03DD004: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 90% Analysis Date = 06/10/14 SpikeMix = Crescent 03DD004: 20 µl & NSI 032614: 20 µl Pct Recovery = 99% Analysis Date = 09/29/15 SpikeMix = Accu 215041380: 25 µl & ERA 0406-15-03: 25 µl Pct Recovery = 91% Analysis Date = 08/15/15 SpikeMix = Supelco LC13545: 25 µl & Crescent 04EE008: 25 µl Pct Recovery = 100% Analysis Date = 07/13/15 SpikeMix = Crescent 04EE008: 25 µl & NSI 050515AVOC: 25 µl Pct Recovery = 100% Analysis Date = 10/13/16 SpikeMix = NSI 041816AVOC: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 100% Analysis Date = 05/27/16 SpikeMix = Phenova B20160319: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 113% Analysis Date = 11/29/16 SpikeMix = ChemService 5082900: 15 µl & Phenova B20160319: 15 µl Pct Recovery = 105% Analysis Date = 09/28/16 SpikeMix = Crescent 03FF058: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 110% Analysis Date = 06/30/16 SpikeMix = ChemService 5082900: 15 µl & Accu 216041125: 15 µl Pct Recovery = 101% Analysis Date = 06/10/16 SpikeMix = NSI 041816AVOC: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 128% Analysis Date = 04/02/16 SpikeMix = Supelco LC13545: 15 µl & Accu 215041380: 15 µl Pct Recovery = 93% Analysis Date = 03/04/16 SpikeMix = Accu 215041380: 15 µl & ERA 0406-15-03: 15 µl Pct Recovery = 80% Analysis Date = 06/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Accu 215041380: 15 µl Pct Recovery = 86% Analysis Date = 01/13/15 SpikeMix = Accu 214031115: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 84% Analysis Date = 09/09/14 SpikeMix = Accu 214031115: 10 µl & NSI 032614: 10 µl Pct Recovery = 103% Analysis Date = 07/23/14 SpikeMix = Spex Organics C1140417015: 10 µl & Accu 214031115: 10 µl Pct Recovery = 99% Analysis Date = 06/18/14 SpikeMix = Supelco LC06438: 10 µl & Accu 214031115: 10 µl Pct Recovery = 90% Analysis Date = 12/18/15 SpikeMix = Supelco LC13545: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 90% Analysis Date = 10/17/15 SpikeMix = Crescent 04EE008: 15 µl & NSI 050515AVOC: 15 µl Pct Recovery = 97% Analysis Date = 05/09/15 SpikeMix = Spex Organics EN150428007: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 105% Analysis Date = 11/06/14 SpikeMix = Spex Organics C1140417015: 10 µl & Crescent 03DD004: 10 µl Pct Recovery = 88% Analysis Date = 10/04/14 SpikeMix = Crescent 03DD004: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 99% Analysis Date = 07/29/14 SpikeMix = Crescent 03DD004: 10 µl & NSI 032614: 10 µl Pct Recovery = 105% Analysis Date = 05/03/14 SpikeMix = Crescent 03DD004: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 103% Analysis Date = 02/18/16 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 84% Analysis Date = 11/20/15 SpikeMix = Accu 215041380: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 89% Analysis Date = 11/12/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 99% Analysis Date = 05/21/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 99% Analysis Date = 05/13/16 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 110% Analysis Date = 01/27/16 SpikeMix = Crescent 04EE008: 10 µl & NSI 050515AVOC: 10 µl Pct Recovery = 112% Analysis Date = 08/07/15 SpikeMix = Crescent 04EE008: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 98% Analysis Date = 05/09/15 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 106% Analysis Date = 12/15/16 Pct Recovery = 107% Analysis Date = 12/11/16 Pct Recovery = 107% Analysis Date = 12/11/16 Pct Recovery = 107% Analysis Date = 12/06/16 Pct Recovery = 107% Analysis Date = 12/06/16 Pct Recovery = 107% Analysis Date = 12/01/16 Pct Recovery = 106% Analysis Date = 12/01/16 Pct Recovery = 106% Analysis Date = 11/26/16 Pct Recovery = 106% Analysis Date = 11/26/16 Pct Recovery = 106% Analysis Date = 11/21/16 Pct Recovery = 106% Analysis Date = 11/21/16 Pct Recovery = 106% Analysis Date = 11/17/16 Pct Recovery = 106% Analysis Date = 11/17/16 Pct Recovery = 106% Analysis Date = 11/12/16 Pct Recovery = 106% Analysis Date = 11/12/16 Pct Recovery = 106% Analysis Date = 11/07/16 Pct Recovery = 106% Analysis Date = 11/07/16 Pct Recovery = 106% Analysis Date = 11/02/16 Pct Recovery = 106% Analysis Date = 11/02/16 Pct Recovery = 106% Analysis Date = 10/28/16 Pct Recovery = 105% Analysis Date = 10/28/16 Pct Recovery = 105% Analysis Date = 10/24/16 Pct Recovery = 105% Analysis Date = 10/24/16 Pct Recovery = 105% Analysis Date = 10/19/16 Pct Recovery = 105% Analysis Date = 10/19/16 Pct Recovery = 105% Analysis Date = 10/14/16 Pct Recovery = 105% Analysis Date = 10/14/16 Pct Recovery = 105% Analysis Date = 10/09/16 Pct Recovery = 105% Analysis Date = 10/09/16 Pct Recovery = 105% Analysis Date = 10/04/16 Pct Recovery = 105% Analysis Date = 10/04/16 Pct Recovery = 105% Analysis Date = 09/30/16 Pct Recovery = 104% Analysis Date = 09/30/16 Pct Recovery = 104% Analysis Date = 09/25/16 Pct Recovery = 104% Analysis Date = 09/25/16 Pct Recovery = 104% Analysis Date = 09/20/16 Pct Recovery = 104% Analysis Date = 09/20/16 Pct Recovery = 104% Analysis Date = 09/15/16 Pct Recovery = 104% Analysis Date = 09/15/16 Pct Recovery = 104% Analysis Date = 09/10/16 Pct Recovery = 104% Analysis Date = 09/10/16 Pct Recovery = 104% Analysis Date = 09/06/16 Pct Recovery = 104% Analysis Date = 09/06/16 Pct Recovery = 104% Analysis Date = 09/01/16 Pct Recovery = 103% Analysis Date = 09/01/16 Pct Recovery = 103% Analysis Date = 08/27/16 Pct Recovery = 103% Analysis Date = 08/27/16 Pct Recovery = 103% Analysis Date = 08/22/16 Pct Recovery = 103% Analysis Date = 08/22/16 Pct Recovery = 103% Analysis Date = 08/17/16 Pct Recovery = 103% Analysis Date = 08/17/16 Pct Recovery = 103% Analysis Date = 08/13/16 Pct Recovery = 103% Analysis Date = 08/13/16 Pct Recovery = 103% Analysis Date = 08/08/16 Pct Recovery = 103% Analysis Date = 08/08/16 Pct Recovery = 103% Analysis Date = 08/03/16 Pct Recovery = 103% Analysis Date = 08/03/16 Pct Recovery = 103% Analysis Date = 07/29/16 Pct Recovery = 102% Analysis Date = 07/29/16 Pct Recovery = 102% Analysis Date = 07/24/16 Pct Recovery = 102% Analysis Date = 07/24/16 Pct Recovery = 102% Analysis Date = 07/20/16 Pct Recovery = 102% Analysis Date = 07/20/16 Pct Recovery = 102% Analysis Date = 07/15/16 Pct Recovery = 102% Analysis Date = 07/15/16 Pct Recovery = 102% Analysis Date = 07/10/16 Pct Recovery = 102% Analysis Date = 07/10/16 Pct Recovery = 102% Analysis Date = 07/05/16 Pct Recovery = 102% Analysis Date = 07/05/16 Pct Recovery = 102% Analysis Date = 06/30/16 Pct Recovery = 101% Analysis Date = 06/30/16 Pct Recovery = 101% Analysis Date = 06/26/16 Pct Recovery = 101% Analysis Date = 06/26/16 Pct Recovery = 101% Analysis Date = 06/21/16 Pct Recovery = 101% Analysis Date = 06/21/16 Pct Recovery = 101% Analysis Date = 06/16/16 Pct Recovery = 101% Analysis Date = 06/16/16 Pct Recovery = 101% Analysis Date = 06/11/16 Pct Recovery = 101% Analysis Date = 06/11/16 Pct Recovery = 101% Analysis Date = 06/06/16 Pct Recovery = 101% Analysis Date = 06/06/16 Pct Recovery = 101% Analysis Date = 06/02/16 Pct Recovery = 100% Analysis Date = 06/02/16 Pct Recovery = 100% Analysis Date = 05/28/16 Pct Recovery = 100% Analysis Date = 05/28/16 Pct Recovery = 100% Analysis Date = 05/23/16 Pct Recovery = 100% Analysis Date = 05/23/16 Pct Recovery = 100% Analysis Date = 05/18/16 Pct Recovery = 100% Analysis Date = 05/18/16 Pct Recovery = 100% Analysis Date = 05/13/16 Pct Recovery = 100% Analysis Date = 05/13/16 Pct Recovery = 100% Analysis Date = 05/09/16 Pct Recovery = 100% Analysis Date = 05/09/16 Pct Recovery = 100% Analysis Date = 05/04/16 Pct Recovery = 100% Analysis Date = 05/04/16 Pct Recovery = 100% Analysis Date = 04/29/16 Pct Recovery = 100% Analysis Date = 04/29/16 Pct Recovery = 100% Analysis Date = 04/24/16 Pct Recovery = 99% Analysis Date = 04/24/16 Pct Recovery = 99% Analysis Date = 04/19/16 Pct Recovery = 99% Analysis Date = 04/19/16 Pct Recovery = 99% Analysis Date = 04/15/16 Pct Recovery = 99% Analysis Date = 04/15/16 Pct Recovery = 99% Analysis Date = 04/10/16 Pct Recovery = 99% Analysis Date = 04/10/16 Pct Recovery = 99% Analysis Date = 04/05/16 Pct Recovery = 99% Analysis Date = 04/05/16 Pct Recovery = 99% Analysis Date = 03/31/16 Pct Recovery = 99% Analysis Date = 03/31/16 Pct Recovery = 99% Analysis Date = 03/26/16 Pct Recovery = 99% Analysis Date = 03/26/16 Pct Recovery = 99% Analysis Date = 03/22/16 Pct Recovery = 99% Analysis Date = 03/22/16 Pct Recovery = 99% Analysis Date = 03/17/16 Pct Recovery = 99% Analysis Date = 03/17/16 Pct Recovery = 99% Analysis Date = 03/12/16 Pct Recovery = 98% Analysis Date = 03/12/16 Pct Recovery = 98% Analysis Date = 03/07/16 Pct Recovery = 98% Analysis Date = 03/07/16 Pct Recovery = 98% Analysis Date = 03/02/16 Pct Recovery = 98% Analysis Date = 03/02/16 Pct Recovery = 98% Analysis Date = 02/27/16 Pct Recovery = 98% Analysis Date = 02/27/16 Pct Recovery = 98% Analysis Date = 02/22/16 Pct Recovery = 98% Analysis Date = 02/22/16 Pct Recovery = 98% Analysis Date = 02/17/16 Pct Recovery = 98% Analysis Date = 02/17/16 Pct Recovery = 98% Analysis Date = 02/12/16 Pct Recovery = 98% Analysis Date = 02/12/16 Pct Recovery = 98% Analysis Date = 02/07/16 Pct Recovery = 98% Analysis Date = 02/07/16 Pct Recovery = 98% Analysis Date = 02/03/16 Pct Recovery = 98% Analysis Date = 02/03/16 Pct Recovery = 98% Analysis Date = 01/29/16 Pct Recovery = 98% Analysis Date = 01/29/16 Pct Recovery = 98% Analysis Date = 01/24/16 Pct Recovery = 98% Analysis Date = 01/24/16 Pct Recovery = 98% Analysis Date = 01/19/16 Pct Recovery = 98% Analysis Date = 01/19/16 Pct Recovery = 98% Analysis Date = 01/14/16 Pct Recovery = 97% Analysis Date = 01/14/16 Pct Recovery = 97% Analysis Date = 01/10/16 Pct Recovery = 97% Analysis Date = 01/10/16 Pct Recovery = 97% Analysis Date = 01/05/16 Pct Recovery = 97% Analysis Date = 01/05/16 Pct Recovery = 97% Analysis Date = 12/31/15 Pct Recovery = 97% Analysis Date = 12/31/15 Pct Recovery = 97% Analysis Date = 12/26/15 Pct Recovery = 97% Analysis Date = 12/26/15 Pct Recovery = 97% Analysis Date = 12/21/15 Pct Recovery = 97% Analysis Date = 12/21/15 Pct Recovery = 97% Analysis Date = 12/17/15 Pct Recovery = 97% Analysis Date = 12/17/15 Pct Recovery = 97% Analysis Date = 12/12/15 Pct Recovery = 97% Analysis Date = 12/12/15 Pct Recovery = 97% Analysis Date = 12/07/15 Pct Recovery = 97% Analysis Date = 12/07/15 Pct Recovery = 97% Analysis Date = 12/02/15 Pct Recovery = 97% Analysis Date = 12/02/15 Pct Recovery = 97% Analysis Date = 11/27/15 Pct Recovery = 97% Analysis Date = 11/27/15 Pct Recovery = 97% Analysis Date = 11/23/15 Pct Recovery = 97% Analysis Date = 11/23/15 Pct Recovery = 97% Analysis Date = 11/18/15 Pct Recovery = 97% Analysis Date = 11/18/15 Pct Recovery = 97% Analysis Date = 11/13/15 Pct Recovery = 97% Analysis Date = 11/13/15 Pct Recovery = 97% Analysis Date = 11/08/15 Pct Recovery = 97% Analysis Date = 11/08/15 Pct Recovery = 97% Analysis Date = 11/03/15 Pct Recovery = 97% Analysis Date = 11/03/15 Pct Recovery = 97% Analysis Date = 10/30/15 Pct Recovery = 97% Analysis Date = 10/30/15 Pct Recovery = 97% Analysis Date = 10/25/15 Pct Recovery = 97% Analysis Date = 10/25/15 Pct Recovery = 97% Analysis Date = 10/20/15 Pct Recovery = 97% Analysis Date = 10/20/15 Pct Recovery = 97% Analysis Date = 10/15/15 Pct Recovery = 97% Analysis Date = 10/15/15 Pct Recovery = 97% Analysis Date = 10/10/15 Pct Recovery = 97% Analysis Date = 10/10/15 Pct Recovery = 97% Analysis Date = 10/06/15 Pct Recovery = 97% Analysis Date = 10/06/15 Pct Recovery = 97% Analysis Date = 10/01/15 Pct Recovery = 97% Analysis Date = 10/01/15 Pct Recovery = 97% Analysis Date = 09/26/15 Pct Recovery = 97% Analysis Date = 09/26/15 Pct Recovery = 97% Analysis Date = 09/21/15 Pct Recovery = 97% Analysis Date = 09/21/15 Pct Recovery = 97% Analysis Date = 09/16/15 Pct Recovery = 97% Analysis Date = 09/16/15 Pct Recovery = 97% Analysis Date = 09/12/15 Pct Recovery = 97% Analysis Date = 09/12/15 Pct Recovery = 97% Analysis Date = 09/07/15 Pct Recovery = 97% Analysis Date = 09/07/15 Pct Recovery = 97% Analysis Date = 09/02/15 Pct Recovery = 97% Analysis Date = 09/02/15 Pct Recovery = 97% Analysis Date = 08/28/15 Pct Recovery = 97% Analysis Date = 08/28/15 Pct Recovery = 97% Analysis Date = 08/23/15 Pct Recovery = 97% Analysis Date = 08/23/15 Pct Recovery = 97% Analysis Date = 08/19/15 Pct Recovery = 97% Analysis Date = 08/19/15 Pct Recovery = 97% Analysis Date = 08/14/15 Pct Recovery = 97% Analysis Date = 08/14/15 Pct Recovery = 97% Analysis Date = 08/09/15 Pct Recovery = 97% Analysis Date = 08/09/15 Pct Recovery = 97% Analysis Date = 08/04/15 Pct Recovery = 97% Analysis Date = 08/04/15 Pct Recovery = 97% Analysis Date = 07/30/15 Pct Recovery = 97% Analysis Date = 07/30/15 Pct Recovery = 97% Analysis Date = 07/26/15 Pct Recovery = 97% Analysis Date = 07/26/15 Pct Recovery = 97% Analysis Date = 07/21/15 Pct Recovery = 97% Analysis Date = 07/21/15 Pct Recovery = 97% Analysis Date = 07/16/15 Pct Recovery = 97% Analysis Date = 07/16/15 Pct Recovery = 97% Analysis Date = 07/11/15 Pct Recovery = 97% Analysis Date = 07/11/15 Pct Recovery = 97% Analysis Date = 07/06/15 Pct Recovery = 97% Analysis Date = 07/06/15 Pct Recovery = 97% Analysis Date = 07/02/15 Pct Recovery = 97% Analysis Date = 07/02/15 Pct Recovery = 97% Analysis Date = 06/27/15 Pct Recovery = 97% Analysis Date = 06/27/15 Pct Recovery = 97% Analysis Date = 06/22/15 Pct Recovery = 97% Analysis Date = 06/22/15 Pct Recovery = 97% Analysis Date = 06/17/15 Pct Recovery = 97% Analysis Date = 06/17/15 Pct Recovery = 97% Analysis Date = 06/12/15 Pct Recovery = 98% Analysis Date = 06/12/15 Pct Recovery = 98% Analysis Date = 06/08/15 Pct Recovery = 98% Analysis Date = 06/08/15 Pct Recovery = 98% Analysis Date = 06/03/15 Pct Recovery = 98% Analysis Date = 06/03/15 Pct Recovery = 98% Analysis Date = 05/29/15 Pct Recovery = 98% Analysis Date = 05/29/15 Pct Recovery = 98% Analysis Date = 05/24/15 Pct Recovery = 98% Analysis Date = 05/24/15 Pct Recovery = 98% Analysis Date = 05/19/15 Pct Recovery = 98% Analysis Date = 05/19/15 Pct Recovery = 98% Analysis Date = 05/15/15 Pct Recovery = 98% Analysis Date = 05/15/15 Pct Recovery = 98% Analysis Date = 05/10/15 Pct Recovery = 98% Analysis Date = 05/10/15 Pct Recovery = 98% Analysis Date = 05/05/15 Pct Recovery = 98% Analysis Date = 05/05/15 Pct Recovery = 98% Analysis Date = 04/30/15 Pct Recovery = 98% Analysis Date = 04/30/15 Pct Recovery = 98% Analysis Date = 04/25/15 Pct Recovery = 98% Analysis Date = 04/25/15 Pct Recovery = 98% Analysis Date = 04/21/15 Pct Recovery = 98% Analysis Date = 04/21/15 Pct Recovery = 98% Analysis Date = 04/16/15 Pct Recovery = 98% Analysis Date = 04/16/15 Pct Recovery = 98% Analysis Date = 04/11/15 Pct Recovery = 98% Analysis Date = 04/11/15 Pct Recovery = 98% Analysis Date = 04/06/15 Pct Recovery = 98% Analysis Date = 04/06/15 Pct Recovery = 98% Analysis Date = 04/01/15 Pct Recovery = 98% Analysis Date = 04/01/15 Pct Recovery = 98% Analysis Date = 03/28/15 Pct Recovery = 98% Analysis Date = 03/28/15 Pct Recovery = 98% Analysis Date = 03/23/15 Pct Recovery = 98% Analysis Date = 03/23/15 Pct Recovery = 98% Analysis Date = 03/18/15 Pct Recovery = 98% Analysis Date = 03/18/15 Pct Recovery = 98% Analysis Date = 03/13/15 Pct Recovery = 98% Analysis Date = 03/13/15 Pct Recovery = 98% Analysis Date = 03/08/15 Pct Recovery = 98% Analysis Date = 03/08/15 Pct Recovery = 98% Analysis Date = 03/04/15 Pct Recovery = 98% Analysis Date = 03/04/15 Pct Recovery = 98% Analysis Date = 02/27/15 Pct Recovery = 98% Analysis Date = 02/27/15 Pct Recovery = 98% Analysis Date = 02/22/15 Pct Recovery = 98% Analysis Date = 02/22/15 Pct Recovery = 98% Analysis Date = 02/17/15 Pct Recovery = 98% Analysis Date = 02/17/15 Pct Recovery = 98% Analysis Date = 02/12/15 Pct Recovery = 98% Analysis Date = 02/12/15 Pct Recovery = 98% Analysis Date = 02/08/15 Pct Recovery = 98% Analysis Date = 02/08/15 Pct Recovery = 98% Analysis Date = 02/03/15 Pct Recovery = 98% Analysis Date = 02/03/15 Pct Recovery = 98% Analysis Date = 01/29/15 Pct Recovery = 98% Analysis Date = 01/29/15 Pct Recovery = 98% Analysis Date = 01/24/15 Pct Recovery = 98% Analysis Date = 01/24/15 Pct Recovery = 98% Analysis Date = 01/19/15 Pct Recovery = 98% Analysis Date = 01/19/15 Pct Recovery = 98% Analysis Date = 01/15/15 Pct Recovery = 98% Analysis Date = 01/15/15 Pct Recovery = 98% Analysis Date = 01/10/15 Pct Recovery = 98% Analysis Date = 01/10/15 Pct Recovery = 98% Analysis Date = 01/05/15 Pct Recovery = 98% Analysis Date = 01/05/15 Pct Recovery = 98% Analysis Date = 12/31/14 Pct Recovery = 98% Analysis Date = 12/31/14 Pct Recovery = 98% Analysis Date = 12/26/14 Pct Recovery = 98% Analysis Date = 12/26/14 Pct Recovery = 98% Analysis Date = 12/22/14 Pct Recovery = 98% Analysis Date = 12/22/14 Pct Recovery = 98% Analysis Date = 12/17/14 Pct Recovery = 98% Analysis Date = 12/17/14 Pct Recovery = 98% Analysis Date = 12/12/14 Pct Recovery = 98% Analysis Date = 12/12/14 Pct Recovery = 98% Analysis Date = 12/07/14 Pct Recovery = 98% Analysis Date = 12/07/14 Pct Recovery = 98% Analysis Date = 12/02/14 Pct Recovery = 98% Analysis Date = 12/02/14 Pct Recovery = 98% Analysis Date = 11/28/14 Pct Recovery = 98% Analysis Date = 11/28/14 Pct Recovery = 98% Analysis Date = 11/23/14 Pct Recovery = 98% Analysis Date = 11/23/14 Pct Recovery = 98% Analysis Date = 11/18/14 Pct Recovery = 98% Analysis Date = 11/18/14 Pct Recovery = 98% Analysis Date = 11/13/14 Pct Recovery = 98% Analysis Date = 11/13/14 Pct Recovery = 98% Analysis Date = 11/08/14 Pct Recovery = 98% Analysis Date = 11/08/14 Pct Recovery = 98% Analysis Date = 11/04/14 Pct Recovery = 98% Analysis Date = 11/04/14 Pct Recovery = 98% Analysis Date = 10/30/14 Pct Recovery = 98% Analysis Date = 10/30/14 Pct Recovery = 98% Analysis Date = 10/25/14 Pct Recovery = 98% Analysis Date = 10/25/14 Pct Recovery = 98% Analysis Date = 10/20/14 Pct Recovery = 98% Analysis Date = 10/20/14 Pct Recovery = 98% Analysis Date = 10/15/14 Pct Recovery = 98% Analysis Date = 10/15/14 Pct Recovery = 98% Analysis Date = 10/11/14 Pct Recovery = 98% Analysis Date = 10/11/14 Pct Recovery = 98% Analysis Date = 10/06/14 Pct Recovery = 98% Analysis Date = 10/06/14 Pct Recovery = 98% Analysis Date = 10/01/14 Pct Recovery = 97% Analysis Date = 10/01/14 Pct Recovery = 97% Analysis Date = 09/26/14 Pct Recovery = 97% Analysis Date = 09/26/14 Pct Recovery = 97% Analysis Date = 09/21/14 Pct Recovery = 97% Analysis Date = 09/21/14 Pct Recovery = 97% Analysis Date = 09/17/14 Pct Recovery = 97% Analysis Date = 09/17/14 Pct Recovery = 97% Analysis Date = 09/12/14 Pct Recovery = 97% Analysis Date = 09/12/14 Pct Recovery = 97% Analysis Date = 09/07/14 Pct Recovery = 97% Analysis Date = 09/07/14 Pct Recovery = 97% Analysis Date = 09/02/14 Pct Recovery = 97% Analysis Date = 09/02/14 Pct Recovery = 97% Analysis Date = 08/28/14 Pct Recovery = 97% Analysis Date = 08/28/14 Pct Recovery = 97% Analysis Date = 08/24/14 Pct Recovery = 97% Analysis Date = 08/24/14 Pct Recovery = 97% Analysis Date = 08/19/14 Pct Recovery = 97% Analysis Date = 08/19/14 Pct Recovery = 97% Analysis Date = 08/14/14 Pct Recovery = 97% Analysis Date = 08/14/14 Pct Recovery = 97% Analysis Date = 08/09/14 Pct Recovery = 97% Analysis Date = 08/09/14 Pct Recovery = 97% Analysis Date = 08/04/14 Pct Recovery = 97% Analysis Date = 08/04/14 Pct Recovery = 97% Analysis Date = 07/31/14 Pct Recovery = 97% Analysis Date = 07/31/14 Pct Recovery = 97% Analysis Date = 07/26/14 Pct Recovery = 97% Analysis Date = 07/26/14 Pct Recovery = 97% Analysis Date = 07/21/14 Pct Recovery = 97% Analysis Date = 07/21/14 Pct Recovery = 97% Analysis Date = 07/16/14 Pct Recovery = 97% Analysis Date = 07/16/14 Pct Recovery = 97% Analysis Date = 07/11/14 Pct Recovery = 97% Analysis Date = 07/11/14 Pct Recovery = 97% Analysis Date = 07/07/14 Pct Recovery = 97% Analysis Date = 07/07/14 Pct Recovery = 97% Analysis Date = 07/02/14 Pct Recovery = 97% Analysis Date = 07/02/14 Pct Recovery = 97% Analysis Date = 06/27/14 Pct Recovery = 97% Analysis Date = 06/27/14 Pct Recovery = 97% Analysis Date = 06/22/14 Pct Recovery = 97% Analysis Date = 06/22/14 Pct Recovery = 97% Analysis Date = 06/17/14 Pct Recovery = 97% Analysis Date = 06/17/14 Pct Recovery = 97% Analysis Date = 06/13/14 Pct Recovery = 97% Analysis Date = 06/13/14 Pct Recovery = 97% Analysis Date = 06/08/14 Pct Recovery = 97% Analysis Date = 06/08/14 Pct Recovery = 97% Analysis Date = 06/03/14 Pct Recovery = 97% Analysis Date = 06/03/14 Pct Recovery = 97% Analysis Date = 05/29/14 Pct Recovery = 97% Analysis Date = 05/29/14 Pct Recovery = 97% Analysis Date = 05/24/14 Pct Recovery = 97% Analysis Date = 05/24/14 Pct Recovery = 97% Analysis Date = 05/20/14 Pct Recovery = 97% Analysis Date = 05/20/14 Pct Recovery = 97% Analysis Date = 05/15/14 Pct Recovery = 97% Analysis Date = 05/15/14 Pct Recovery = 97% Analysis Date = 05/10/14 Pct Recovery = 97% Analysis Date = 05/10/14 Pct Recovery = 97% Analysis Date = 05/05/14 Pct Recovery = 97% Analysis Date = 05/05/14 Pct Recovery = 97% Analysis Date = 05/01/14 Pct Recovery = 97% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
1,2-DICHLOROPROPANE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 47 99% 11% 99% 11%
Total 47 99% 11% 99% 11%

Sample Statistics
1,2-DICHLOROPROPANE

Characteristic N % % Basis
Plotted 47 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 47 .  
False Negatives 0 0% 0 out of 47
Not Spiked 26 .  
False Positives 1 4% 1 out of 26

BQS OBSP Determination:
1,3,5-TRIMETHYLBENZENE
METHOD: 4440 , TESTIDCODE: 77226GCM66
Open Data Set

Analysis Date = 12/16/16 SpikeMix = NSI 041816AVOC: 40 µl & ChemService 5082900: 40 µl Pct Recovery = 90% Analysis Date = 08/04/16 SpikeMix = Crescent 03FF058: 40 µl & Supelco LC20141V: 40 µl Pct Recovery = 85% Analysis Date = 07/20/16 SpikeMix = Supelco LC20141V: 40 µl & Accu 216041125: 40 µl Pct Recovery = 94% Analysis Date = 11/21/16 SpikeMix = Crescent 03FF058: 25 µl & Supelco LC20141V: 25 µl Pct Recovery = 87% Analysis Date = 09/08/16 SpikeMix = Supelco LC20141V: 25 µl & Accu 216041125: 25 µl Pct Recovery = 84% Analysis Date = 08/26/16 SpikeMix = NSI 041816AVOC: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 85% Analysis Date = 08/12/16 SpikeMix = ChemService 5082900: 25 µl & Phenova B20160319: 25 µl Pct Recovery = 94% Analysis Date = 06/30/16 SpikeMix = Crescent 03FF058: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 87% Analysis Date = 03/19/15 SpikeMix = Spex Organics C1140417015: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 105% Analysis Date = 12/17/14 SpikeMix = Supelco LC06438: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 94% Analysis Date = 11/14/14 SpikeMix = Crescent 03DD004: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 83% Analysis Date = 06/10/14 SpikeMix = Crescent 03DD004: 20 µl & NSI 032614: 20 µl Pct Recovery = 77% Analysis Date = 08/15/15 SpikeMix = Supelco LC13545: 25 µl & Crescent 04EE008: 25 µl Pct Recovery = 96% Analysis Date = 06/16/15 SpikeMix = ERA 0406-15-03: 25 µl & Supelco LC13545: 25 µl Pct Recovery = 82% Analysis Date = 04/09/15 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 78% Analysis Date = 08/19/14 SpikeMix = Spex Organics C1140417015: 20 µl & Accu 214031115: 20 µl Pct Recovery = 99% Analysis Date = 07/01/14 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 82% Analysis Date = 05/01/14 SpikeMix = Accu 214031115: 20 µl & NSI 032614: 20 µl Pct Recovery = 72% Analysis Date = 11/29/16 SpikeMix = ChemService 5082900: 15 µl & Phenova B20160319: 15 µl Pct Recovery = 99% Analysis Date = 10/13/16 SpikeMix = NSI 041816AVOC: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 83% Analysis Date = 09/28/16 SpikeMix = Crescent 03FF058: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 92% Analysis Date = 06/30/16 SpikeMix = ChemService 5082900: 15 µl & Accu 216041125: 15 µl Pct Recovery = 87% Analysis Date = 06/10/16 SpikeMix = NSI 041816AVOC: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 93% Analysis Date = 05/27/16 SpikeMix = Phenova B20160319: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 94% Analysis Date = 04/26/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 84% Analysis Date = 04/02/16 SpikeMix = Supelco LC13545: 15 µl & Accu 215041380: 15 µl Pct Recovery = 90% Analysis Date = 02/05/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 94% Analysis Date = 12/18/15 SpikeMix = Supelco LC13545: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 91% Analysis Date = 11/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 95% Analysis Date = 10/16/15 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 92% Analysis Date = 05/09/15 SpikeMix = Spex Organics EN150428007: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 102% Analysis Date = 11/06/14 SpikeMix = Spex Organics C1140417015: 10 µl & Crescent 03DD004: 10 µl Pct Recovery = 100% Analysis Date = 10/04/14 SpikeMix = Crescent 03DD004: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 89% Analysis Date = 07/29/14 SpikeMix = Crescent 03DD004: 10 µl & NSI 032614: 10 µl Pct Recovery = 90% Analysis Date = 05/03/14 SpikeMix = Crescent 03DD004: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 103% Analysis Date = 01/13/15 SpikeMix = Accu 214031115: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 90% Analysis Date = 09/09/14 SpikeMix = Accu 214031115: 10 µl & NSI 032614: 10 µl Pct Recovery = 108% Analysis Date = 07/23/14 SpikeMix = Spex Organics C1140417015: 10 µl & Accu 214031115: 10 µl Pct Recovery = 106% Analysis Date = 06/18/14 SpikeMix = Supelco LC06438: 10 µl & Accu 214031115: 10 µl Pct Recovery = 84% Analysis Date = 05/13/16 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 97% Analysis Date = 03/17/16 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 79% Analysis Date = 02/18/16 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 96% Analysis Date = 12/10/15 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 90% Analysis Date = 11/12/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 99% Analysis Date = 09/03/15 SpikeMix = NSI 050515AVOC: 10 µl & Spex Organics EN150428007: 10 µl Pct Recovery = 85% Analysis Date = 06/27/15 SpikeMix = ERA 0406-15-03: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 99% Analysis Date = 05/21/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 107% Analysis Date = 05/09/15 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 104% Analysis Date = 12/15/16 Pct Recovery = 89% Analysis Date = 12/11/16 Pct Recovery = 89% Analysis Date = 12/11/16 Pct Recovery = 89% Analysis Date = 12/06/16 Pct Recovery = 89% Analysis Date = 12/06/16 Pct Recovery = 89% Analysis Date = 12/01/16 Pct Recovery = 89% Analysis Date = 12/01/16 Pct Recovery = 89% Analysis Date = 11/26/16 Pct Recovery = 89% Analysis Date = 11/26/16 Pct Recovery = 89% Analysis Date = 11/21/16 Pct Recovery = 89% Analysis Date = 11/21/16 Pct Recovery = 89% Analysis Date = 11/17/16 Pct Recovery = 89% Analysis Date = 11/17/16 Pct Recovery = 89% Analysis Date = 11/12/16 Pct Recovery = 89% Analysis Date = 11/12/16 Pct Recovery = 89% Analysis Date = 11/07/16 Pct Recovery = 89% Analysis Date = 11/07/16 Pct Recovery = 89% Analysis Date = 11/02/16 Pct Recovery = 89% Analysis Date = 11/02/16 Pct Recovery = 89% Analysis Date = 10/28/16 Pct Recovery = 89% Analysis Date = 10/28/16 Pct Recovery = 89% Analysis Date = 10/24/16 Pct Recovery = 89% Analysis Date = 10/24/16 Pct Recovery = 89% Analysis Date = 10/19/16 Pct Recovery = 89% Analysis Date = 10/19/16 Pct Recovery = 89% Analysis Date = 10/14/16 Pct Recovery = 89% Analysis Date = 10/14/16 Pct Recovery = 89% Analysis Date = 10/09/16 Pct Recovery = 89% Analysis Date = 10/09/16 Pct Recovery = 89% Analysis Date = 10/04/16 Pct Recovery = 89% Analysis Date = 10/04/16 Pct Recovery = 89% Analysis Date = 09/30/16 Pct Recovery = 89% Analysis Date = 09/30/16 Pct Recovery = 89% Analysis Date = 09/25/16 Pct Recovery = 89% Analysis Date = 09/25/16 Pct Recovery = 89% Analysis Date = 09/20/16 Pct Recovery = 89% Analysis Date = 09/20/16 Pct Recovery = 89% Analysis Date = 09/15/16 Pct Recovery = 89% Analysis Date = 09/15/16 Pct Recovery = 89% Analysis Date = 09/10/16 Pct Recovery = 89% Analysis Date = 09/10/16 Pct Recovery = 89% Analysis Date = 09/06/16 Pct Recovery = 89% Analysis Date = 09/06/16 Pct Recovery = 89% Analysis Date = 09/01/16 Pct Recovery = 89% Analysis Date = 09/01/16 Pct Recovery = 89% Analysis Date = 08/27/16 Pct Recovery = 89% Analysis Date = 08/27/16 Pct Recovery = 89% Analysis Date = 08/22/16 Pct Recovery = 89% Analysis Date = 08/22/16 Pct Recovery = 89% Analysis Date = 08/17/16 Pct Recovery = 89% Analysis Date = 08/17/16 Pct Recovery = 89% Analysis Date = 08/13/16 Pct Recovery = 89% Analysis Date = 08/13/16 Pct Recovery = 89% Analysis Date = 08/08/16 Pct Recovery = 90% Analysis Date = 08/08/16 Pct Recovery = 90% Analysis Date = 08/03/16 Pct Recovery = 90% Analysis Date = 08/03/16 Pct Recovery = 90% Analysis Date = 07/29/16 Pct Recovery = 90% Analysis Date = 07/29/16 Pct Recovery = 90% Analysis Date = 07/24/16 Pct Recovery = 90% Analysis Date = 07/24/16 Pct Recovery = 90% Analysis Date = 07/20/16 Pct Recovery = 90% Analysis Date = 07/20/16 Pct Recovery = 90% Analysis Date = 07/15/16 Pct Recovery = 90% Analysis Date = 07/15/16 Pct Recovery = 90% Analysis Date = 07/10/16 Pct Recovery = 90% Analysis Date = 07/10/16 Pct Recovery = 90% Analysis Date = 07/05/16 Pct Recovery = 90% Analysis Date = 07/05/16 Pct Recovery = 90% Analysis Date = 06/30/16 Pct Recovery = 90% Analysis Date = 06/30/16 Pct Recovery = 90% Analysis Date = 06/26/16 Pct Recovery = 90% Analysis Date = 06/26/16 Pct Recovery = 90% Analysis Date = 06/21/16 Pct Recovery = 90% Analysis Date = 06/21/16 Pct Recovery = 90% Analysis Date = 06/16/16 Pct Recovery = 90% Analysis Date = 06/16/16 Pct Recovery = 90% Analysis Date = 06/11/16 Pct Recovery = 90% Analysis Date = 06/11/16 Pct Recovery = 90% Analysis Date = 06/06/16 Pct Recovery = 90% Analysis Date = 06/06/16 Pct Recovery = 90% Analysis Date = 06/02/16 Pct Recovery = 90% Analysis Date = 06/02/16 Pct Recovery = 90% Analysis Date = 05/28/16 Pct Recovery = 90% Analysis Date = 05/28/16 Pct Recovery = 90% Analysis Date = 05/23/16 Pct Recovery = 90% Analysis Date = 05/23/16 Pct Recovery = 90% Analysis Date = 05/18/16 Pct Recovery = 90% Analysis Date = 05/18/16 Pct Recovery = 90% Analysis Date = 05/13/16 Pct Recovery = 90% Analysis Date = 05/13/16 Pct Recovery = 90% Analysis Date = 05/09/16 Pct Recovery = 90% Analysis Date = 05/09/16 Pct Recovery = 90% Analysis Date = 05/04/16 Pct Recovery = 90% Analysis Date = 05/04/16 Pct Recovery = 90% Analysis Date = 04/29/16 Pct Recovery = 90% Analysis Date = 04/29/16 Pct Recovery = 90% Analysis Date = 04/24/16 Pct Recovery = 90% Analysis Date = 04/24/16 Pct Recovery = 90% Analysis Date = 04/19/16 Pct Recovery = 90% Analysis Date = 04/19/16 Pct Recovery = 90% Analysis Date = 04/15/16 Pct Recovery = 90% Analysis Date = 04/15/16 Pct Recovery = 90% Analysis Date = 04/10/16 Pct Recovery = 91% Analysis Date = 04/10/16 Pct Recovery = 91% Analysis Date = 04/05/16 Pct Recovery = 91% Analysis Date = 04/05/16 Pct Recovery = 91% Analysis Date = 03/31/16 Pct Recovery = 91% Analysis Date = 03/31/16 Pct Recovery = 91% Analysis Date = 03/26/16 Pct Recovery = 91% Analysis Date = 03/26/16 Pct Recovery = 91% Analysis Date = 03/22/16 Pct Recovery = 91% Analysis Date = 03/22/16 Pct Recovery = 91% Analysis Date = 03/17/16 Pct Recovery = 91% Analysis Date = 03/17/16 Pct Recovery = 91% Analysis Date = 03/12/16 Pct Recovery = 91% Analysis Date = 03/12/16 Pct Recovery = 91% Analysis Date = 03/07/16 Pct Recovery = 91% Analysis Date = 03/07/16 Pct Recovery = 91% Analysis Date = 03/02/16 Pct Recovery = 91% Analysis Date = 03/02/16 Pct Recovery = 91% Analysis Date = 02/27/16 Pct Recovery = 91% Analysis Date = 02/27/16 Pct Recovery = 91% Analysis Date = 02/22/16 Pct Recovery = 91% Analysis Date = 02/22/16 Pct Recovery = 91% Analysis Date = 02/17/16 Pct Recovery = 91% Analysis Date = 02/17/16 Pct Recovery = 91% Analysis Date = 02/12/16 Pct Recovery = 91% Analysis Date = 02/12/16 Pct Recovery = 91% Analysis Date = 02/07/16 Pct Recovery = 91% Analysis Date = 02/07/16 Pct Recovery = 91% Analysis Date = 02/03/16 Pct Recovery = 91% Analysis Date = 02/03/16 Pct Recovery = 91% Analysis Date = 01/29/16 Pct Recovery = 91% Analysis Date = 01/29/16 Pct Recovery = 91% Analysis Date = 01/24/16 Pct Recovery = 91% Analysis Date = 01/24/16 Pct Recovery = 91% Analysis Date = 01/19/16 Pct Recovery = 92% Analysis Date = 01/19/16 Pct Recovery = 92% Analysis Date = 01/14/16 Pct Recovery = 92% Analysis Date = 01/14/16 Pct Recovery = 92% Analysis Date = 01/10/16 Pct Recovery = 92% Analysis Date = 01/10/16 Pct Recovery = 92% Analysis Date = 01/05/16 Pct Recovery = 92% Analysis Date = 01/05/16 Pct Recovery = 92% Analysis Date = 12/31/15 Pct Recovery = 92% Analysis Date = 12/31/15 Pct Recovery = 92% Analysis Date = 12/26/15 Pct Recovery = 92% Analysis Date = 12/26/15 Pct Recovery = 92% Analysis Date = 12/21/15 Pct Recovery = 92% Analysis Date = 12/21/15 Pct Recovery = 92% Analysis Date = 12/17/15 Pct Recovery = 92% Analysis Date = 12/17/15 Pct Recovery = 92% Analysis Date = 12/12/15 Pct Recovery = 92% Analysis Date = 12/12/15 Pct Recovery = 92% Analysis Date = 12/07/15 Pct Recovery = 92% Analysis Date = 12/07/15 Pct Recovery = 92% Analysis Date = 12/02/15 Pct Recovery = 92% Analysis Date = 12/02/15 Pct Recovery = 92% Analysis Date = 11/27/15 Pct Recovery = 92% Analysis Date = 11/27/15 Pct Recovery = 92% Analysis Date = 11/23/15 Pct Recovery = 92% Analysis Date = 11/23/15 Pct Recovery = 92% Analysis Date = 11/18/15 Pct Recovery = 93% Analysis Date = 11/18/15 Pct Recovery = 93% Analysis Date = 11/13/15 Pct Recovery = 93% Analysis Date = 11/13/15 Pct Recovery = 93% Analysis Date = 11/08/15 Pct Recovery = 93% Analysis Date = 11/08/15 Pct Recovery = 93% Analysis Date = 11/03/15 Pct Recovery = 93% Analysis Date = 11/03/15 Pct Recovery = 93% Analysis Date = 10/30/15 Pct Recovery = 93% Analysis Date = 10/30/15 Pct Recovery = 93% Analysis Date = 10/25/15 Pct Recovery = 93% Analysis Date = 10/25/15 Pct Recovery = 93% Analysis Date = 10/20/15 Pct Recovery = 93% Analysis Date = 10/20/15 Pct Recovery = 93% Analysis Date = 10/15/15 Pct Recovery = 93% Analysis Date = 10/15/15 Pct Recovery = 93% Analysis Date = 10/10/15 Pct Recovery = 93% Analysis Date = 10/10/15 Pct Recovery = 93% Analysis Date = 10/06/15 Pct Recovery = 93% Analysis Date = 10/06/15 Pct Recovery = 93% Analysis Date = 10/01/15 Pct Recovery = 93% Analysis Date = 10/01/15 Pct Recovery = 93% Analysis Date = 09/26/15 Pct Recovery = 93% Analysis Date = 09/26/15 Pct Recovery = 93% Analysis Date = 09/21/15 Pct Recovery = 93% Analysis Date = 09/21/15 Pct Recovery = 93% Analysis Date = 09/16/15 Pct Recovery = 93% Analysis Date = 09/16/15 Pct Recovery = 93% Analysis Date = 09/12/15 Pct Recovery = 94% Analysis Date = 09/12/15 Pct Recovery = 94% Analysis Date = 09/07/15 Pct Recovery = 94% Analysis Date = 09/07/15 Pct Recovery = 94% Analysis Date = 09/02/15 Pct Recovery = 94% Analysis Date = 09/02/15 Pct Recovery = 94% Analysis Date = 08/28/15 Pct Recovery = 94% Analysis Date = 08/28/15 Pct Recovery = 94% Analysis Date = 08/23/15 Pct Recovery = 94% Analysis Date = 08/23/15 Pct Recovery = 94% Analysis Date = 08/19/15 Pct Recovery = 94% Analysis Date = 08/19/15 Pct Recovery = 94% Analysis Date = 08/14/15 Pct Recovery = 94% Analysis Date = 08/14/15 Pct Recovery = 94% Analysis Date = 08/09/15 Pct Recovery = 94% Analysis Date = 08/09/15 Pct Recovery = 94% Analysis Date = 08/04/15 Pct Recovery = 94% Analysis Date = 08/04/15 Pct Recovery = 94% Analysis Date = 07/30/15 Pct Recovery = 94% Analysis Date = 07/30/15 Pct Recovery = 94% Analysis Date = 07/26/15 Pct Recovery = 94% Analysis Date = 07/26/15 Pct Recovery = 94% Analysis Date = 07/21/15 Pct Recovery = 94% Analysis Date = 07/21/15 Pct Recovery = 94% Analysis Date = 07/16/15 Pct Recovery = 94% Analysis Date = 07/16/15 Pct Recovery = 94% Analysis Date = 07/11/15 Pct Recovery = 94% Analysis Date = 07/11/15 Pct Recovery = 94% Analysis Date = 07/06/15 Pct Recovery = 94% Analysis Date = 07/06/15 Pct Recovery = 94% Analysis Date = 07/02/15 Pct Recovery = 94% Analysis Date = 07/02/15 Pct Recovery = 94% Analysis Date = 06/27/15 Pct Recovery = 94% Analysis Date = 06/27/15 Pct Recovery = 94% Analysis Date = 06/22/15 Pct Recovery = 94% Analysis Date = 06/22/15 Pct Recovery = 94% Analysis Date = 06/17/15 Pct Recovery = 94% Analysis Date = 06/17/15 Pct Recovery = 94% Analysis Date = 06/12/15 Pct Recovery = 94% Analysis Date = 06/12/15 Pct Recovery = 94% Analysis Date = 06/08/15 Pct Recovery = 94% Analysis Date = 06/08/15 Pct Recovery = 94% Analysis Date = 06/03/15 Pct Recovery = 94% Analysis Date = 06/03/15 Pct Recovery = 94% Analysis Date = 05/29/15 Pct Recovery = 94% Analysis Date = 05/29/15 Pct Recovery = 94% Analysis Date = 05/24/15 Pct Recovery = 94% Analysis Date = 05/24/15 Pct Recovery = 94% Analysis Date = 05/19/15 Pct Recovery = 94% Analysis Date = 05/19/15 Pct Recovery = 94% Analysis Date = 05/15/15 Pct Recovery = 94% Analysis Date = 05/15/15 Pct Recovery = 94% Analysis Date = 05/10/15 Pct Recovery = 95% Analysis Date = 05/10/15 Pct Recovery = 95% Analysis Date = 05/05/15 Pct Recovery = 95% Analysis Date = 05/05/15 Pct Recovery = 95% Analysis Date = 04/30/15 Pct Recovery = 95% Analysis Date = 04/30/15 Pct Recovery = 95% Analysis Date = 04/25/15 Pct Recovery = 95% Analysis Date = 04/25/15 Pct Recovery = 95% Analysis Date = 04/21/15 Pct Recovery = 95% Analysis Date = 04/21/15 Pct Recovery = 95% Analysis Date = 04/16/15 Pct Recovery = 95% Analysis Date = 04/16/15 Pct Recovery = 95% Analysis Date = 04/11/15 Pct Recovery = 95% Analysis Date = 04/11/15 Pct Recovery = 95% Analysis Date = 04/06/15 Pct Recovery = 95% Analysis Date = 04/06/15 Pct Recovery = 95% Analysis Date = 04/01/15 Pct Recovery = 95% Analysis Date = 04/01/15 Pct Recovery = 95% Analysis Date = 03/28/15 Pct Recovery = 95% Analysis Date = 03/28/15 Pct Recovery = 95% Analysis Date = 03/23/15 Pct Recovery = 95% Analysis Date = 03/23/15 Pct Recovery = 95% Analysis Date = 03/18/15 Pct Recovery = 95% Analysis Date = 03/18/15 Pct Recovery = 95% Analysis Date = 03/13/15 Pct Recovery = 95% Analysis Date = 03/13/15 Pct Recovery = 95% Analysis Date = 03/08/15 Pct Recovery = 95% Analysis Date = 03/08/15 Pct Recovery = 95% Analysis Date = 03/04/15 Pct Recovery = 95% Analysis Date = 03/04/15 Pct Recovery = 95% Analysis Date = 02/27/15 Pct Recovery = 94% Analysis Date = 02/27/15 Pct Recovery = 94% Analysis Date = 02/22/15 Pct Recovery = 94% Analysis Date = 02/22/15 Pct Recovery = 94% Analysis Date = 02/17/15 Pct Recovery = 94% Analysis Date = 02/17/15 Pct Recovery = 94% Analysis Date = 02/12/15 Pct Recovery = 94% Analysis Date = 02/12/15 Pct Recovery = 94% Analysis Date = 02/08/15 Pct Recovery = 94% Analysis Date = 02/08/15 Pct Recovery = 94% Analysis Date = 02/03/15 Pct Recovery = 94% Analysis Date = 02/03/15 Pct Recovery = 94% Analysis Date = 01/29/15 Pct Recovery = 94% Analysis Date = 01/29/15 Pct Recovery = 94% Analysis Date = 01/24/15 Pct Recovery = 94% Analysis Date = 01/24/15 Pct Recovery = 94% Analysis Date = 01/19/15 Pct Recovery = 94% Analysis Date = 01/19/15 Pct Recovery = 94% Analysis Date = 01/15/15 Pct Recovery = 94% Analysis Date = 01/15/15 Pct Recovery = 94% Analysis Date = 01/10/15 Pct Recovery = 94% Analysis Date = 01/10/15 Pct Recovery = 94% Analysis Date = 01/05/15 Pct Recovery = 94% Analysis Date = 01/05/15 Pct Recovery = 94% Analysis Date = 12/31/14 Pct Recovery = 94% Analysis Date = 12/31/14 Pct Recovery = 94% Analysis Date = 12/26/14 Pct Recovery = 94% Analysis Date = 12/26/14 Pct Recovery = 94% Analysis Date = 12/22/14 Pct Recovery = 94% Analysis Date = 12/22/14 Pct Recovery = 94% Analysis Date = 12/17/14 Pct Recovery = 93% Analysis Date = 12/17/14 Pct Recovery = 93% Analysis Date = 12/12/14 Pct Recovery = 93% Analysis Date = 12/12/14 Pct Recovery = 93% Analysis Date = 12/07/14 Pct Recovery = 93% Analysis Date = 12/07/14 Pct Recovery = 93% Analysis Date = 12/02/14 Pct Recovery = 93% Analysis Date = 12/02/14 Pct Recovery = 93% Analysis Date = 11/28/14 Pct Recovery = 93% Analysis Date = 11/28/14 Pct Recovery = 93% Analysis Date = 11/23/14 Pct Recovery = 93% Analysis Date = 11/23/14 Pct Recovery = 93% Analysis Date = 11/18/14 Pct Recovery = 93% Analysis Date = 11/18/14 Pct Recovery = 93% Analysis Date = 11/13/14 Pct Recovery = 93% Analysis Date = 11/13/14 Pct Recovery = 93% Analysis Date = 11/08/14 Pct Recovery = 93% Analysis Date = 11/08/14 Pct Recovery = 93% Analysis Date = 11/04/14 Pct Recovery = 93% Analysis Date = 11/04/14 Pct Recovery = 93% Analysis Date = 10/30/14 Pct Recovery = 93% Analysis Date = 10/30/14 Pct Recovery = 93% Analysis Date = 10/25/14 Pct Recovery = 93% Analysis Date = 10/25/14 Pct Recovery = 93% Analysis Date = 10/20/14 Pct Recovery = 92% Analysis Date = 10/20/14 Pct Recovery = 92% Analysis Date = 10/15/14 Pct Recovery = 92% Analysis Date = 10/15/14 Pct Recovery = 92% Analysis Date = 10/11/14 Pct Recovery = 92% Analysis Date = 10/11/14 Pct Recovery = 92% Analysis Date = 10/06/14 Pct Recovery = 92% Analysis Date = 10/06/14 Pct Recovery = 92% Analysis Date = 10/01/14 Pct Recovery = 92% Analysis Date = 10/01/14 Pct Recovery = 92% Analysis Date = 09/26/14 Pct Recovery = 92% Analysis Date = 09/26/14 Pct Recovery = 92% Analysis Date = 09/21/14 Pct Recovery = 92% Analysis Date = 09/21/14 Pct Recovery = 92% Analysis Date = 09/17/14 Pct Recovery = 92% Analysis Date = 09/17/14 Pct Recovery = 92% Analysis Date = 09/12/14 Pct Recovery = 92% Analysis Date = 09/12/14 Pct Recovery = 92% Analysis Date = 09/07/14 Pct Recovery = 91% Analysis Date = 09/07/14 Pct Recovery = 91% Analysis Date = 09/02/14 Pct Recovery = 91% Analysis Date = 09/02/14 Pct Recovery = 91% Analysis Date = 08/28/14 Pct Recovery = 91% Analysis Date = 08/28/14 Pct Recovery = 91% Analysis Date = 08/24/14 Pct Recovery = 91% Analysis Date = 08/24/14 Pct Recovery = 91% Analysis Date = 08/19/14 Pct Recovery = 91% Analysis Date = 08/19/14 Pct Recovery = 91% Analysis Date = 08/14/14 Pct Recovery = 91% Analysis Date = 08/14/14 Pct Recovery = 91% Analysis Date = 08/09/14 Pct Recovery = 91% Analysis Date = 08/09/14 Pct Recovery = 91% Analysis Date = 08/04/14 Pct Recovery = 91% Analysis Date = 08/04/14 Pct Recovery = 91% Analysis Date = 07/31/14 Pct Recovery = 91% Analysis Date = 07/31/14 Pct Recovery = 91% Analysis Date = 07/26/14 Pct Recovery = 91% Analysis Date = 07/26/14 Pct Recovery = 91% Analysis Date = 07/21/14 Pct Recovery = 90% Analysis Date = 07/21/14 Pct Recovery = 90% Analysis Date = 07/16/14 Pct Recovery = 90% Analysis Date = 07/16/14 Pct Recovery = 90% Analysis Date = 07/11/14 Pct Recovery = 90% Analysis Date = 07/11/14 Pct Recovery = 90% Analysis Date = 07/07/14 Pct Recovery = 90% Analysis Date = 07/07/14 Pct Recovery = 90% Analysis Date = 07/02/14 Pct Recovery = 90% Analysis Date = 07/02/14 Pct Recovery = 90% Analysis Date = 06/27/14 Pct Recovery = 90% Analysis Date = 06/27/14 Pct Recovery = 90% Analysis Date = 06/22/14 Pct Recovery = 90% Analysis Date = 06/22/14 Pct Recovery = 90% Analysis Date = 06/17/14 Pct Recovery = 90% Analysis Date = 06/17/14 Pct Recovery = 90% Analysis Date = 06/13/14 Pct Recovery = 90% Analysis Date = 06/13/14 Pct Recovery = 90% Analysis Date = 06/08/14 Pct Recovery = 89% Analysis Date = 06/08/14 Pct Recovery = 89% Analysis Date = 06/03/14 Pct Recovery = 89% Analysis Date = 06/03/14 Pct Recovery = 89% Analysis Date = 05/29/14 Pct Recovery = 89% Analysis Date = 05/29/14 Pct Recovery = 89% Analysis Date = 05/24/14 Pct Recovery = 89% Analysis Date = 05/24/14 Pct Recovery = 89% Analysis Date = 05/20/14 Pct Recovery = 89% Analysis Date = 05/20/14 Pct Recovery = 89% Analysis Date = 05/15/14 Pct Recovery = 89% Analysis Date = 05/15/14 Pct Recovery = 89% Analysis Date = 05/10/14 Pct Recovery = 89% Analysis Date = 05/10/14 Pct Recovery = 89% Analysis Date = 05/05/14 Pct Recovery = 89% Analysis Date = 05/05/14 Pct Recovery = 89% Analysis Date = 05/01/14 Pct Recovery = 88% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
1,3,5-TRIMETHYLBENZENE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 48 92% 9% 91% 10%
Total 48 92% 9% 91% 10%

Sample Statistics
1,3,5-TRIMETHYLBENZENE

Characteristic N % % Basis
Plotted 48 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 48 .  
False Negatives 0 0% 0 out of 48
Not Spiked 25 .  
False Positives 0 0% 0 out of 25

BQS OBSP Determination:
1,3-BUTADIENE
METHOD: 4440 , TESTIDCODE: 68726GCM66
Open Data Set

Analysis Date = 12/12/16 SpikeMix = Accu 216041125: 40 µl & Crescent 03FF058: 40 µl Pct Recovery = 93% Analysis Date = 08/04/16 SpikeMix = Crescent 03FF058: 40 µl & Supelco LC20141V: 40 µl Pct Recovery = 75% Analysis Date = 11/21/16 SpikeMix = Crescent 03FF058: 25 µl & Supelco LC20141V: 25 µl Pct Recovery = 58% Analysis Date = 06/30/16 SpikeMix = Crescent 03FF058: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 70% Analysis Date = 06/21/16 SpikeMix = Phenova B20160319: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 79% Analysis Date = 05/24/16 SpikeMix = Accu 216041125: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 70% Analysis Date = 03/19/15 SpikeMix = Spex Organics C1140417015: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 100% Analysis Date = 03/06/15 SpikeMix = ERA 0227-14-06.1A: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 93% Analysis Date = 12/17/14 SpikeMix = Supelco LC06438: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 97% Analysis Date = 11/22/14 SpikeMix = NSI 032614: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 100% Analysis Date = 09/21/14 SpikeMix = Supelco LC06438: 20 µl Pct Recovery = 98% Analysis Date = 08/19/14 SpikeMix = Spex Organics C1140417015: 20 µl & Accu 214031115: 20 µl Pct Recovery = 113% Analysis Date = 08/16/14 SpikeMix = ERA 0227-14-06.1A: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 112% Analysis Date = 06/10/14 SpikeMix = NSI 032614: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 111% Analysis Date = 08/15/15 SpikeMix = Supelco LC13545: 25 µl & Crescent 04EE008: 25 µl Pct Recovery = 109% Analysis Date = 06/16/15 SpikeMix = ERA 0406-15-03: 25 µl & Supelco LC13545: 25 µl Pct Recovery = 88% Analysis Date = 09/28/16 SpikeMix = Crescent 03FF058: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 42% Analysis Date = 09/08/16 SpikeMix = Phenova B20160319: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 92% Analysis Date = 08/20/16 SpikeMix = Accu 216041125: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 89% Analysis Date = 04/26/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 68% Analysis Date = 04/02/16 SpikeMix = Supelco LC13545: 15 µl & Accu 215041380: 15 µl Pct Recovery = 103% Analysis Date = 02/05/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 91% Analysis Date = 12/18/15 SpikeMix = Supelco LC13545: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 99% Analysis Date = 11/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 83% Analysis Date = 10/16/15 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 87% Analysis Date = 05/09/15 SpikeMix = Spex Organics EN150428007: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 160% Analysis Date = 11/06/14 SpikeMix = Spex Organics C1140417015: 10 µl & Crescent 03DD004: 10 µl Pct Recovery = 107% Analysis Date = 10/21/14 SpikeMix = ERA 0227-14-06.1A: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 83% Analysis Date = 09/09/14 SpikeMix = NSI 032614: 10 µl & Spex Organics C1140417015: 10 µl Pct Recovery = 111% Analysis Date = 07/23/14 SpikeMix = Spex Organics C1140417015: 10 µl & Accu 214031115: 10 µl Pct Recovery = 134% Analysis Date = 07/11/14 SpikeMix = Spex Organics C1140417015: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 151% Analysis Date = 06/18/14 SpikeMix = Supelco LC06438: 10 µl & Accu 214031115: 10 µl Pct Recovery = 108% Analysis Date = 05/30/14 SpikeMix = NSI 032614: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 124% Analysis Date = 05/03/14 SpikeMix = Crescent 03DD004: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 114% Analysis Date = 05/13/16 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 70% Analysis Date = 03/17/16 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 84% Analysis Date = 02/18/16 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 110% Analysis Date = 12/10/15 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 98% Analysis Date = 11/12/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 124% Analysis Date = 09/03/15 SpikeMix = NSI 050515AVOC: 10 µl & Spex Organics EN150428007: 10 µl Pct Recovery = 75% Analysis Date = 06/27/15 SpikeMix = ERA 0406-15-03: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 93% Analysis Date = 05/21/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 136% Analysis Date = 05/09/15 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 144% Analysis Date = 12/12/16 Pct Recovery = 67% Analysis Date = 12/07/16 Pct Recovery = 68% Analysis Date = 12/07/16 Pct Recovery = 68% Analysis Date = 12/02/16 Pct Recovery = 68% Analysis Date = 12/02/16 Pct Recovery = 68% Analysis Date = 11/27/16 Pct Recovery = 68% Analysis Date = 11/27/16 Pct Recovery = 68% Analysis Date = 11/22/16 Pct Recovery = 69% Analysis Date = 11/22/16 Pct Recovery = 69% Analysis Date = 11/18/16 Pct Recovery = 69% Analysis Date = 11/18/16 Pct Recovery = 69% Analysis Date = 11/13/16 Pct Recovery = 69% Analysis Date = 11/13/16 Pct Recovery = 69% Analysis Date = 11/08/16 Pct Recovery = 70% Analysis Date = 11/08/16 Pct Recovery = 70% Analysis Date = 11/03/16 Pct Recovery = 70% Analysis Date = 11/03/16 Pct Recovery = 70% Analysis Date = 10/30/16 Pct Recovery = 70% Analysis Date = 10/30/16 Pct Recovery = 70% Analysis Date = 10/25/16 Pct Recovery = 71% Analysis Date = 10/25/16 Pct Recovery = 71% Analysis Date = 10/20/16 Pct Recovery = 71% Analysis Date = 10/20/16 Pct Recovery = 71% Analysis Date = 10/15/16 Pct Recovery = 71% Analysis Date = 10/15/16 Pct Recovery = 71% Analysis Date = 10/10/16 Pct Recovery = 72% Analysis Date = 10/10/16 Pct Recovery = 72% Analysis Date = 10/06/16 Pct Recovery = 72% Analysis Date = 10/06/16 Pct Recovery = 72% Analysis Date = 10/01/16 Pct Recovery = 72% Analysis Date = 10/01/16 Pct Recovery = 72% Analysis Date = 09/26/16 Pct Recovery = 73% Analysis Date = 09/26/16 Pct Recovery = 73% Analysis Date = 09/21/16 Pct Recovery = 73% Analysis Date = 09/21/16 Pct Recovery = 73% Analysis Date = 09/17/16 Pct Recovery = 73% Analysis Date = 09/17/16 Pct Recovery = 73% Analysis Date = 09/12/16 Pct Recovery = 74% Analysis Date = 09/12/16 Pct Recovery = 74% Analysis Date = 09/07/16 Pct Recovery = 74% Analysis Date = 09/07/16 Pct Recovery = 74% Analysis Date = 09/02/16 Pct Recovery = 74% Analysis Date = 09/02/16 Pct Recovery = 74% Analysis Date = 08/29/16 Pct Recovery = 75% Analysis Date = 08/29/16 Pct Recovery = 75% Analysis Date = 08/24/16 Pct Recovery = 75% Analysis Date = 08/24/16 Pct Recovery = 75% Analysis Date = 08/19/16 Pct Recovery = 75% Analysis Date = 08/19/16 Pct Recovery = 75% Analysis Date = 08/14/16 Pct Recovery = 76% Analysis Date = 08/14/16 Pct Recovery = 76% Analysis Date = 08/09/16 Pct Recovery = 76% Analysis Date = 08/09/16 Pct Recovery = 76% Analysis Date = 08/05/16 Pct Recovery = 76% Analysis Date = 08/05/16 Pct Recovery = 76% Analysis Date = 07/31/16 Pct Recovery = 77% Analysis Date = 07/31/16 Pct Recovery = 77% Analysis Date = 07/26/16 Pct Recovery = 77% Analysis Date = 07/26/16 Pct Recovery = 77% Analysis Date = 07/21/16 Pct Recovery = 77% Analysis Date = 07/21/16 Pct Recovery = 77% Analysis Date = 07/17/16 Pct Recovery = 78% Analysis Date = 07/17/16 Pct Recovery = 78% Analysis Date = 07/12/16 Pct Recovery = 78% Analysis Date = 07/12/16 Pct Recovery = 78% Analysis Date = 07/07/16 Pct Recovery = 78% Analysis Date = 07/07/16 Pct Recovery = 78% Analysis Date = 07/02/16 Pct Recovery = 79% Analysis Date = 07/02/16 Pct Recovery = 79% Analysis Date = 06/28/16 Pct Recovery = 79% Analysis Date = 06/28/16 Pct Recovery = 79% Analysis Date = 06/23/16 Pct Recovery = 80% Analysis Date = 06/23/16 Pct Recovery = 80% Analysis Date = 06/18/16 Pct Recovery = 80% Analysis Date = 06/18/16 Pct Recovery = 80% Analysis Date = 06/13/16 Pct Recovery = 80% Analysis Date = 06/13/16 Pct Recovery = 80% Analysis Date = 06/08/16 Pct Recovery = 81% Analysis Date = 06/08/16 Pct Recovery = 81% Analysis Date = 06/04/16 Pct Recovery = 81% Analysis Date = 06/04/16 Pct Recovery = 81% Analysis Date = 05/30/16 Pct Recovery = 81% Analysis Date = 05/30/16 Pct Recovery = 81% Analysis Date = 05/25/16 Pct Recovery = 82% Analysis Date = 05/25/16 Pct Recovery = 82% Analysis Date = 05/20/16 Pct Recovery = 82% Analysis Date = 05/20/16 Pct Recovery = 82% Analysis Date = 05/16/16 Pct Recovery = 82% Analysis Date = 05/16/16 Pct Recovery = 82% Analysis Date = 05/11/16 Pct Recovery = 83% Analysis Date = 05/11/16 Pct Recovery = 83% Analysis Date = 05/06/16 Pct Recovery = 83% Analysis Date = 05/06/16 Pct Recovery = 83% Analysis Date = 05/01/16 Pct Recovery = 83% Analysis Date = 05/01/16 Pct Recovery = 83% Analysis Date = 04/27/16 Pct Recovery = 84% Analysis Date = 04/27/16 Pct Recovery = 84% Analysis Date = 04/22/16 Pct Recovery = 84% Analysis Date = 04/22/16 Pct Recovery = 84% Analysis Date = 04/17/16 Pct Recovery = 84% Analysis Date = 04/17/16 Pct Recovery = 84% Analysis Date = 04/12/16 Pct Recovery = 85% Analysis Date = 04/12/16 Pct Recovery = 85% Analysis Date = 04/07/16 Pct Recovery = 85% Analysis Date = 04/07/16 Pct Recovery = 85% Analysis Date = 04/03/16 Pct Recovery = 85% Analysis Date = 04/03/16 Pct Recovery = 85% Analysis Date = 03/29/16 Pct Recovery = 86% Analysis Date = 03/29/16 Pct Recovery = 86% Analysis Date = 03/24/16 Pct Recovery = 86% Analysis Date = 03/24/16 Pct Recovery = 86% Analysis Date = 03/19/16 Pct Recovery = 87% Analysis Date = 03/19/16 Pct Recovery = 87% Analysis Date = 03/15/16 Pct Recovery = 87% Analysis Date = 03/15/16 Pct Recovery = 87% Analysis Date = 03/10/16 Pct Recovery = 87% Analysis Date = 03/10/16 Pct Recovery = 87% Analysis Date = 03/05/16 Pct Recovery = 88% Analysis Date = 03/05/16 Pct Recovery = 88% Analysis Date = 02/29/16 Pct Recovery = 88% Analysis Date = 02/29/16 Pct Recovery = 88% Analysis Date = 02/25/16 Pct Recovery = 88% Analysis Date = 02/25/16 Pct Recovery = 88% Analysis Date = 02/20/16 Pct Recovery = 89% Analysis Date = 02/20/16 Pct Recovery = 89% Analysis Date = 02/15/16 Pct Recovery = 89% Analysis Date = 02/15/16 Pct Recovery = 89% Analysis Date = 02/10/16 Pct Recovery = 89% Analysis Date = 02/10/16 Pct Recovery = 89% Analysis Date = 02/05/16 Pct Recovery = 90% Analysis Date = 02/05/16 Pct Recovery = 90% Analysis Date = 02/01/16 Pct Recovery = 90% Analysis Date = 02/01/16 Pct Recovery = 90% Analysis Date = 01/27/16 Pct Recovery = 91% Analysis Date = 01/27/16 Pct Recovery = 91% Analysis Date = 01/22/16 Pct Recovery = 91% Analysis Date = 01/22/16 Pct Recovery = 91% Analysis Date = 01/17/16 Pct Recovery = 91% Analysis Date = 01/17/16 Pct Recovery = 91% Analysis Date = 01/13/16 Pct Recovery = 92% Analysis Date = 01/13/16 Pct Recovery = 92% Analysis Date = 01/08/16 Pct Recovery = 92% Analysis Date = 01/08/16 Pct Recovery = 92% Analysis Date = 01/03/16 Pct Recovery = 92% Analysis Date = 01/03/16 Pct Recovery = 92% Analysis Date = 12/29/15 Pct Recovery = 93% Analysis Date = 12/29/15 Pct Recovery = 93% Analysis Date = 12/25/15 Pct Recovery = 93% Analysis Date = 12/25/15 Pct Recovery = 93% Analysis Date = 12/20/15 Pct Recovery = 94% Analysis Date = 12/20/15 Pct Recovery = 94% Analysis Date = 12/15/15 Pct Recovery = 94% Analysis Date = 12/15/15 Pct Recovery = 94% Analysis Date = 12/10/15 Pct Recovery = 95% Analysis Date = 12/10/15 Pct Recovery = 95% Analysis Date = 12/05/15 Pct Recovery = 95% Analysis Date = 12/05/15 Pct Recovery = 95% Analysis Date = 12/01/15 Pct Recovery = 96% Analysis Date = 12/01/15 Pct Recovery = 96% Analysis Date = 11/26/15 Pct Recovery = 96% Analysis Date = 11/26/15 Pct Recovery = 96% Analysis Date = 11/21/15 Pct Recovery = 97% Analysis Date = 11/21/15 Pct Recovery = 97% Analysis Date = 11/16/15 Pct Recovery = 97% Analysis Date = 11/16/15 Pct Recovery = 97% Analysis Date = 11/12/15 Pct Recovery = 98% Analysis Date = 11/12/15 Pct Recovery = 98% Analysis Date = 11/07/15 Pct Recovery = 99% Analysis Date = 11/07/15 Pct Recovery = 99% Analysis Date = 11/02/15 Pct Recovery = 99% Analysis Date = 11/02/15 Pct Recovery = 99% Analysis Date = 10/28/15 Pct Recovery = 99% Analysis Date = 10/28/15 Pct Recovery = 99% Analysis Date = 10/24/15 Pct Recovery = 100% Analysis Date = 10/24/15 Pct Recovery = 100% Analysis Date = 10/19/15 Pct Recovery = 100% Analysis Date = 10/19/15 Pct Recovery = 100% Analysis Date = 10/14/15 Pct Recovery = 101% Analysis Date = 10/14/15 Pct Recovery = 101% Analysis Date = 10/09/15 Pct Recovery = 101% Analysis Date = 10/09/15 Pct Recovery = 101% Analysis Date = 10/04/15 Pct Recovery = 102% Analysis Date = 10/04/15 Pct Recovery = 102% Analysis Date = 09/30/15 Pct Recovery = 102% Analysis Date = 09/30/15 Pct Recovery = 102% Analysis Date = 09/25/15 Pct Recovery = 102% Analysis Date = 09/25/15 Pct Recovery = 102% Analysis Date = 09/20/15 Pct Recovery = 103% Analysis Date = 09/20/15 Pct Recovery = 103% Analysis Date = 09/15/15 Pct Recovery = 103% Analysis Date = 09/15/15 Pct Recovery = 103% Analysis Date = 09/11/15 Pct Recovery = 104% Analysis Date = 09/11/15 Pct Recovery = 104% Analysis Date = 09/06/15 Pct Recovery = 104% Analysis Date = 09/06/15 Pct Recovery = 104% Analysis Date = 09/01/15 Pct Recovery = 104% Analysis Date = 09/01/15 Pct Recovery = 104% Analysis Date = 08/27/15 Pct Recovery = 105% Analysis Date = 08/27/15 Pct Recovery = 105% Analysis Date = 08/23/15 Pct Recovery = 105% Analysis Date = 08/23/15 Pct Recovery = 105% Analysis Date = 08/18/15 Pct Recovery = 106% Analysis Date = 08/18/15 Pct Recovery = 106% Analysis Date = 08/13/15 Pct Recovery = 106% Analysis Date = 08/13/15 Pct Recovery = 106% Analysis Date = 08/08/15 Pct Recovery = 106% Analysis Date = 08/08/15 Pct Recovery = 106% Analysis Date = 08/03/15 Pct Recovery = 106% Analysis Date = 08/03/15 Pct Recovery = 106% Analysis Date = 07/30/15 Pct Recovery = 106% Analysis Date = 07/30/15 Pct Recovery = 106% Analysis Date = 07/25/15 Pct Recovery = 106% Analysis Date = 07/25/15 Pct Recovery = 106% Analysis Date = 07/20/15 Pct Recovery = 106% Analysis Date = 07/20/15 Pct Recovery = 106% Analysis Date = 07/15/15 Pct Recovery = 106% Analysis Date = 07/15/15 Pct Recovery = 106% Analysis Date = 07/11/15 Pct Recovery = 106% Analysis Date = 07/11/15 Pct Recovery = 106% Analysis Date = 07/06/15 Pct Recovery = 107% Analysis Date = 07/06/15 Pct Recovery = 107% Analysis Date = 07/01/15 Pct Recovery = 107% Analysis Date = 07/01/15 Pct Recovery = 107% Analysis Date = 06/26/15 Pct Recovery = 107% Analysis Date = 06/26/15 Pct Recovery = 107% Analysis Date = 06/21/15 Pct Recovery = 107% Analysis Date = 06/21/15 Pct Recovery = 107% Analysis Date = 06/17/15 Pct Recovery = 107% Analysis Date = 06/17/15 Pct Recovery = 107% Analysis Date = 06/12/15 Pct Recovery = 107% Analysis Date = 06/12/15 Pct Recovery = 107% Analysis Date = 06/07/15 Pct Recovery = 107% Analysis Date = 06/07/15 Pct Recovery = 107% Analysis Date = 06/02/15 Pct Recovery = 107% Analysis Date = 06/02/15 Pct Recovery = 107% Analysis Date = 05/29/15 Pct Recovery = 107% Analysis Date = 05/29/15 Pct Recovery = 107% Analysis Date = 05/24/15 Pct Recovery = 107% Analysis Date = 05/24/15 Pct Recovery = 107% Analysis Date = 05/19/15 Pct Recovery = 107% Analysis Date = 05/19/15 Pct Recovery = 107% Analysis Date = 05/14/15 Pct Recovery = 107% Analysis Date = 05/14/15 Pct Recovery = 107% Analysis Date = 05/10/15 Pct Recovery = 108% Analysis Date = 05/10/15 Pct Recovery = 108% Analysis Date = 05/05/15 Pct Recovery = 108% Analysis Date = 05/05/15 Pct Recovery = 108% Analysis Date = 04/30/15 Pct Recovery = 108% Analysis Date = 04/30/15 Pct Recovery = 108% Analysis Date = 04/25/15 Pct Recovery = 108% Analysis Date = 04/25/15 Pct Recovery = 108% Analysis Date = 04/20/15 Pct Recovery = 108% Analysis Date = 04/20/15 Pct Recovery = 108% Analysis Date = 04/16/15 Pct Recovery = 108% Analysis Date = 04/16/15 Pct Recovery = 108% Analysis Date = 04/11/15 Pct Recovery = 108% Analysis Date = 04/11/15 Pct Recovery = 108% Analysis Date = 04/06/15 Pct Recovery = 108% Analysis Date = 04/06/15 Pct Recovery = 108% Analysis Date = 04/01/15 Pct Recovery = 109% Analysis Date = 04/01/15 Pct Recovery = 109% Analysis Date = 03/28/15 Pct Recovery = 109% Analysis Date = 03/28/15 Pct Recovery = 109% Analysis Date = 03/23/15 Pct Recovery = 109% Analysis Date = 03/23/15 Pct Recovery = 109% Analysis Date = 03/18/15 Pct Recovery = 109% Analysis Date = 03/18/15 Pct Recovery = 109% Analysis Date = 03/13/15 Pct Recovery = 109% Analysis Date = 03/13/15 Pct Recovery = 109% Analysis Date = 03/09/15 Pct Recovery = 109% Analysis Date = 03/09/15 Pct Recovery = 109% Analysis Date = 03/04/15 Pct Recovery = 109% Analysis Date = 03/04/15 Pct Recovery = 109% Analysis Date = 02/27/15 Pct Recovery = 110% Analysis Date = 02/27/15 Pct Recovery = 110% Analysis Date = 02/22/15 Pct Recovery = 110% Analysis Date = 02/22/15 Pct Recovery = 110% Analysis Date = 02/17/15 Pct Recovery = 110% Analysis Date = 02/17/15 Pct Recovery = 110% Analysis Date = 02/13/15 Pct Recovery = 110% Analysis Date = 02/13/15 Pct Recovery = 110% Analysis Date = 02/08/15 Pct Recovery = 110% Analysis Date = 02/08/15 Pct Recovery = 110% Analysis Date = 02/03/15 Pct Recovery = 110% Analysis Date = 02/03/15 Pct Recovery = 110% Analysis Date = 01/29/15 Pct Recovery = 110% Analysis Date = 01/29/15 Pct Recovery = 110% Analysis Date = 01/25/15 Pct Recovery = 110% Analysis Date = 01/25/15 Pct Recovery = 110% Analysis Date = 01/20/15 Pct Recovery = 111% Analysis Date = 01/20/15 Pct Recovery = 111% Analysis Date = 01/15/15 Pct Recovery = 111% Analysis Date = 01/15/15 Pct Recovery = 111% Analysis Date = 01/10/15 Pct Recovery = 111% Analysis Date = 01/10/15 Pct Recovery = 111% Analysis Date = 01/06/15 Pct Recovery = 111% Analysis Date = 01/06/15 Pct Recovery = 111% Analysis Date = 01/01/15 Pct Recovery = 111% Analysis Date = 01/01/15 Pct Recovery = 111% Analysis Date = 12/27/14 Pct Recovery = 111% Analysis Date = 12/27/14 Pct Recovery = 111% Analysis Date = 12/22/14 Pct Recovery = 111% Analysis Date = 12/22/14 Pct Recovery = 111% Analysis Date = 12/17/14 Pct Recovery = 112% Analysis Date = 12/17/14 Pct Recovery = 112% Analysis Date = 12/13/14 Pct Recovery = 112% Analysis Date = 12/13/14 Pct Recovery = 112% Analysis Date = 12/08/14 Pct Recovery = 112% Analysis Date = 12/08/14 Pct Recovery = 112% Analysis Date = 12/03/14 Pct Recovery = 112% Analysis Date = 12/03/14 Pct Recovery = 112% Analysis Date = 11/28/14 Pct Recovery = 112% Analysis Date = 11/28/14 Pct Recovery = 112% Analysis Date = 11/24/14 Pct Recovery = 112% Analysis Date = 11/24/14 Pct Recovery = 112% Analysis Date = 11/19/14 Pct Recovery = 112% Analysis Date = 11/19/14 Pct Recovery = 112% Analysis Date = 11/14/14 Pct Recovery = 112% Analysis Date = 11/14/14 Pct Recovery = 112% Analysis Date = 11/09/14 Pct Recovery = 112% Analysis Date = 11/09/14 Pct Recovery = 112% Analysis Date = 11/05/14 Pct Recovery = 112% Analysis Date = 11/05/14 Pct Recovery = 112% Analysis Date = 10/31/14 Pct Recovery = 112% Analysis Date = 10/31/14 Pct Recovery = 112% Analysis Date = 10/26/14 Pct Recovery = 112% Analysis Date = 10/26/14 Pct Recovery = 112% Analysis Date = 10/21/14 Pct Recovery = 112% Analysis Date = 10/21/14 Pct Recovery = 112% Analysis Date = 10/16/14 Pct Recovery = 113% Analysis Date = 10/16/14 Pct Recovery = 113% Analysis Date = 10/12/14 Pct Recovery = 113% Analysis Date = 10/12/14 Pct Recovery = 113% Analysis Date = 10/07/14 Pct Recovery = 113% Analysis Date = 10/07/14 Pct Recovery = 113% Analysis Date = 10/02/14 Pct Recovery = 113% Analysis Date = 10/02/14 Pct Recovery = 113% Analysis Date = 09/27/14 Pct Recovery = 113% Analysis Date = 09/27/14 Pct Recovery = 113% Analysis Date = 09/23/14 Pct Recovery = 113% Analysis Date = 09/23/14 Pct Recovery = 113% Analysis Date = 09/18/14 Pct Recovery = 113% Analysis Date = 09/18/14 Pct Recovery = 113% Analysis Date = 09/13/14 Pct Recovery = 113% Analysis Date = 09/13/14 Pct Recovery = 113% Analysis Date = 09/08/14 Pct Recovery = 113% Analysis Date = 09/08/14 Pct Recovery = 113% Analysis Date = 09/04/14 Pct Recovery = 113% Analysis Date = 09/04/14 Pct Recovery = 113% Analysis Date = 08/30/14 Pct Recovery = 113% Analysis Date = 08/30/14 Pct Recovery = 113% Analysis Date = 08/25/14 Pct Recovery = 114% Analysis Date = 08/25/14 Pct Recovery = 114% Analysis Date = 08/20/14 Pct Recovery = 114% Analysis Date = 08/20/14 Pct Recovery = 114% Analysis Date = 08/15/14 Pct Recovery = 114% Analysis Date = 08/15/14 Pct Recovery = 114% Analysis Date = 08/11/14 Pct Recovery = 114% Analysis Date = 08/11/14 Pct Recovery = 114% Analysis Date = 08/06/14 Pct Recovery = 114% Analysis Date = 08/06/14 Pct Recovery = 114% Analysis Date = 08/01/14 Pct Recovery = 114% Analysis Date = 08/01/14 Pct Recovery = 114% Analysis Date = 07/27/14 Pct Recovery = 114% Analysis Date = 07/27/14 Pct Recovery = 114% Analysis Date = 07/23/14 Pct Recovery = 114% Analysis Date = 07/23/14 Pct Recovery = 114% Analysis Date = 07/18/14 Pct Recovery = 114% Analysis Date = 07/18/14 Pct Recovery = 114% Analysis Date = 07/13/14 Pct Recovery = 114% Analysis Date = 07/13/14 Pct Recovery = 114% Analysis Date = 07/08/14 Pct Recovery = 115% Analysis Date = 07/08/14 Pct Recovery = 115% Analysis Date = 07/04/14 Pct Recovery = 115% Analysis Date = 07/04/14 Pct Recovery = 115% Analysis Date = 06/29/14 Pct Recovery = 115% Analysis Date = 06/29/14 Pct Recovery = 115% Analysis Date = 06/24/14 Pct Recovery = 115% Analysis Date = 06/24/14 Pct Recovery = 115% Analysis Date = 06/19/14 Pct Recovery = 115% Analysis Date = 06/19/14 Pct Recovery = 115% Analysis Date = 06/14/14 Pct Recovery = 115% Analysis Date = 06/14/14 Pct Recovery = 115% Analysis Date = 06/10/14 Pct Recovery = 115% Analysis Date = 06/10/14 Pct Recovery = 115% Analysis Date = 06/05/14 Pct Recovery = 116% Analysis Date = 06/05/14 Pct Recovery = 116% Analysis Date = 05/31/14 Pct Recovery = 116% Analysis Date = 05/31/14 Pct Recovery = 116% Analysis Date = 05/26/14 Pct Recovery = 116% Analysis Date = 05/26/14 Pct Recovery = 116% Analysis Date = 05/22/14 Pct Recovery = 116% Analysis Date = 05/22/14 Pct Recovery = 116% Analysis Date = 05/17/14 Pct Recovery = 116% Analysis Date = 05/17/14 Pct Recovery = 116% Analysis Date = 05/12/14 Pct Recovery = 117% Analysis Date = 05/12/14 Pct Recovery = 117% Analysis Date = 05/07/14 Pct Recovery = 117% Analysis Date = 05/07/14 Pct Recovery = 117% Analysis Date = 05/03/14 Pct Recovery = 117% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
1,3-BUTADIENE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 43 99% 24% 98% 21%
Total 43 99% 24% 98% 21%

Sample Statistics
1,3-BUTADIENE

Characteristic N % % Basis
Plotted 43 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 43 .  
False Negatives 0 0% 0 out of 43
Not Spiked 23 .  
False Positives 8 35% 8 out of 23

BQS OBSP Determination:
1,3-DICHLOROBENZENE
METHOD: 4440 , TESTIDCODE: 34566GCM66
Open Data Set

Analysis Date = 12/12/16 SpikeMix = Accu 216041125: 40 µl & Crescent 03FF058: 40 µl Pct Recovery = 108% Analysis Date = 08/04/16 SpikeMix = Crescent 03FF058: 40 µl & Supelco LC20141V: 40 µl Pct Recovery = 94% Analysis Date = 11/21/16 SpikeMix = Crescent 03FF058: 25 µl & Supelco LC20141V: 25 µl Pct Recovery = 96% Analysis Date = 06/30/16 SpikeMix = Crescent 03FF058: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 98% Analysis Date = 06/21/16 SpikeMix = Phenova B20160319: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 107% Analysis Date = 05/24/16 SpikeMix = Accu 216041125: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 98% Analysis Date = 04/09/15 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 88% Analysis Date = 03/06/15 SpikeMix = ERA 0227-14-06.1A: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 100% Analysis Date = 11/14/14 SpikeMix = Crescent 03DD004: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 95% Analysis Date = 08/16/14 SpikeMix = ERA 0227-14-06.1A: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 88% Analysis Date = 07/01/14 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 89% Analysis Date = 11/22/14 SpikeMix = NSI 032614: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 99% Analysis Date = 06/10/14 SpikeMix = Crescent 03DD004: 20 µl & NSI 032614: 20 µl Pct Recovery = 82% Analysis Date = 06/10/14 SpikeMix = NSI 032614: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 100% Analysis Date = 05/01/14 SpikeMix = Accu 214031115: 20 µl & NSI 032614: 20 µl Pct Recovery = 81% Analysis Date = 08/15/15 SpikeMix = Supelco LC13545: 25 µl & Crescent 04EE008: 25 µl Pct Recovery = 107% Analysis Date = 07/13/15 SpikeMix = Crescent 04EE008: 25 µl & NSI 050515AVOC: 25 µl Pct Recovery = 84% Analysis Date = 09/29/15 SpikeMix = Accu 215041380: 25 µl & ERA 0406-15-03: 25 µl Pct Recovery = 78% Analysis Date = 09/28/16 SpikeMix = Crescent 03FF058: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 88% Analysis Date = 09/08/16 SpikeMix = Phenova B20160319: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 95% Analysis Date = 08/20/16 SpikeMix = Accu 216041125: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 102% Analysis Date = 12/18/15 SpikeMix = Supelco LC13545: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 107% Analysis Date = 10/17/15 SpikeMix = Crescent 04EE008: 15 µl & NSI 050515AVOC: 15 µl Pct Recovery = 92% Analysis Date = 05/09/15 SpikeMix = Spex Organics EN150428007: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 102% Analysis Date = 04/02/16 SpikeMix = Supelco LC13545: 15 µl & Accu 215041380: 15 µl Pct Recovery = 86% Analysis Date = 03/04/16 SpikeMix = Accu 215041380: 15 µl & ERA 0406-15-03: 15 µl Pct Recovery = 81% Analysis Date = 06/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Accu 215041380: 15 µl Pct Recovery = 75% Analysis Date = 01/13/15 SpikeMix = Accu 214031115: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 97% Analysis Date = 10/21/14 SpikeMix = ERA 0227-14-06.1A: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 97% Analysis Date = 10/04/14 SpikeMix = Crescent 03DD004: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 101% Analysis Date = 07/11/14 SpikeMix = Spex Organics C1140417015: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 90% Analysis Date = 09/09/14 SpikeMix = Accu 214031115: 10 µl & NSI 032614: 10 µl Pct Recovery = 102% Analysis Date = 09/09/14 SpikeMix = NSI 032614: 10 µl & Spex Organics C1140417015: 10 µl Pct Recovery = 96% Analysis Date = 07/29/14 SpikeMix = Crescent 03DD004: 10 µl & NSI 032614: 10 µl Pct Recovery = 83% Analysis Date = 05/30/14 SpikeMix = NSI 032614: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 75% Analysis Date = 05/13/16 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 100% Analysis Date = 01/27/16 SpikeMix = Crescent 04EE008: 10 µl & NSI 050515AVOC: 10 µl Pct Recovery = 105% Analysis Date = 07/31/15 SpikeMix = Crescent 04EE008: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 100% Analysis Date = 05/09/15 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 96% Analysis Date = 02/18/16 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 85% Analysis Date = 11/20/15 SpikeMix = Accu 215041380: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 87% Analysis Date = 11/12/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 80% Analysis Date = 05/21/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 98% Analysis Date = 12/11/16 Pct Recovery = 100% Analysis Date = 12/07/16 Pct Recovery = 100% Analysis Date = 12/07/16 Pct Recovery = 100% Analysis Date = 12/02/16 Pct Recovery = 100% Analysis Date = 12/02/16 Pct Recovery = 100% Analysis Date = 11/27/16 Pct Recovery = 100% Analysis Date = 11/27/16 Pct Recovery = 100% Analysis Date = 11/22/16 Pct Recovery = 100% Analysis Date = 11/22/16 Pct Recovery = 100% Analysis Date = 11/18/16 Pct Recovery = 100% Analysis Date = 11/18/16 Pct Recovery = 100% Analysis Date = 11/13/16 Pct Recovery = 100% Analysis Date = 11/13/16 Pct Recovery = 100% Analysis Date = 11/08/16 Pct Recovery = 100% Analysis Date = 11/08/16 Pct Recovery = 100% Analysis Date = 11/03/16 Pct Recovery = 99% Analysis Date = 11/03/16 Pct Recovery = 99% Analysis Date = 10/29/16 Pct Recovery = 99% Analysis Date = 10/29/16 Pct Recovery = 99% Analysis Date = 10/25/16 Pct Recovery = 99% Analysis Date = 10/25/16 Pct Recovery = 99% Analysis Date = 10/20/16 Pct Recovery = 99% Analysis Date = 10/20/16 Pct Recovery = 99% Analysis Date = 10/15/16 Pct Recovery = 99% Analysis Date = 10/15/16 Pct Recovery = 99% Analysis Date = 10/10/16 Pct Recovery = 99% Analysis Date = 10/10/16 Pct Recovery = 99% Analysis Date = 10/06/16 Pct Recovery = 99% Analysis Date = 10/06/16 Pct Recovery = 99% Analysis Date = 10/01/16 Pct Recovery = 99% Analysis Date = 10/01/16 Pct Recovery = 99% Analysis Date = 09/26/16 Pct Recovery = 98% Analysis Date = 09/26/16 Pct Recovery = 98% Analysis Date = 09/21/16 Pct Recovery = 98% Analysis Date = 09/21/16 Pct Recovery = 98% Analysis Date = 09/16/16 Pct Recovery = 98% Analysis Date = 09/16/16 Pct Recovery = 98% Analysis Date = 09/12/16 Pct Recovery = 98% Analysis Date = 09/12/16 Pct Recovery = 98% Analysis Date = 09/07/16 Pct Recovery = 98% Analysis Date = 09/07/16 Pct Recovery = 98% Analysis Date = 09/02/16 Pct Recovery = 98% Analysis Date = 09/02/16 Pct Recovery = 98% Analysis Date = 08/28/16 Pct Recovery = 98% Analysis Date = 08/28/16 Pct Recovery = 98% Analysis Date = 08/24/16 Pct Recovery = 98% Analysis Date = 08/24/16 Pct Recovery = 98% Analysis Date = 08/19/16 Pct Recovery = 98% Analysis Date = 08/19/16 Pct Recovery = 98% Analysis Date = 08/14/16 Pct Recovery = 97% Analysis Date = 08/14/16 Pct Recovery = 97% Analysis Date = 08/09/16 Pct Recovery = 97% Analysis Date = 08/09/16 Pct Recovery = 97% Analysis Date = 08/04/16 Pct Recovery = 97% Analysis Date = 08/04/16 Pct Recovery = 97% Analysis Date = 07/31/16 Pct Recovery = 97% Analysis Date = 07/31/16 Pct Recovery = 97% Analysis Date = 07/26/16 Pct Recovery = 97% Analysis Date = 07/26/16 Pct Recovery = 97% Analysis Date = 07/21/16 Pct Recovery = 97% Analysis Date = 07/21/16 Pct Recovery = 97% Analysis Date = 07/16/16 Pct Recovery = 97% Analysis Date = 07/16/16 Pct Recovery = 97% Analysis Date = 07/12/16 Pct Recovery = 97% Analysis Date = 07/12/16 Pct Recovery = 97% Analysis Date = 07/07/16 Pct Recovery = 96% Analysis Date = 07/07/16 Pct Recovery = 96% Analysis Date = 07/02/16 Pct Recovery = 96% Analysis Date = 07/02/16 Pct Recovery = 96% Analysis Date = 06/27/16 Pct Recovery = 96% Analysis Date = 06/27/16 Pct Recovery = 96% Analysis Date = 06/22/16 Pct Recovery = 96% Analysis Date = 06/22/16 Pct Recovery = 96% Analysis Date = 06/18/16 Pct Recovery = 96% Analysis Date = 06/18/16 Pct Recovery = 96% Analysis Date = 06/13/16 Pct Recovery = 96% Analysis Date = 06/13/16 Pct Recovery = 96% Analysis Date = 06/08/16 Pct Recovery = 96% Analysis Date = 06/08/16 Pct Recovery = 96% Analysis Date = 06/03/16 Pct Recovery = 96% Analysis Date = 06/03/16 Pct Recovery = 96% Analysis Date = 05/30/16 Pct Recovery = 96% Analysis Date = 05/30/16 Pct Recovery = 96% Analysis Date = 05/25/16 Pct Recovery = 95% Analysis Date = 05/25/16 Pct Recovery = 95% Analysis Date = 05/20/16 Pct Recovery = 95% Analysis Date = 05/20/16 Pct Recovery = 95% Analysis Date = 05/15/16 Pct Recovery = 95% Analysis Date = 05/15/16 Pct Recovery = 95% Analysis Date = 05/10/16 Pct Recovery = 95% Analysis Date = 05/10/16 Pct Recovery = 95% Analysis Date = 05/06/16 Pct Recovery = 95% Analysis Date = 05/06/16 Pct Recovery = 95% Analysis Date = 05/01/16 Pct Recovery = 95% Analysis Date = 05/01/16 Pct Recovery = 95% Analysis Date = 04/26/16 Pct Recovery = 95% Analysis Date = 04/26/16 Pct Recovery = 95% Analysis Date = 04/21/16 Pct Recovery = 95% Analysis Date = 04/21/16 Pct Recovery = 95% Analysis Date = 04/16/16 Pct Recovery = 95% Analysis Date = 04/16/16 Pct Recovery = 95% Analysis Date = 04/12/16 Pct Recovery = 94% Analysis Date = 04/12/16 Pct Recovery = 94% Analysis Date = 04/07/16 Pct Recovery = 94% Analysis Date = 04/07/16 Pct Recovery = 94% Analysis Date = 04/02/16 Pct Recovery = 94% Analysis Date = 04/02/16 Pct Recovery = 94% Analysis Date = 03/28/16 Pct Recovery = 94% Analysis Date = 03/28/16 Pct Recovery = 94% Analysis Date = 03/24/16 Pct Recovery = 94% Analysis Date = 03/24/16 Pct Recovery = 94% Analysis Date = 03/19/16 Pct Recovery = 94% Analysis Date = 03/19/16 Pct Recovery = 94% Analysis Date = 03/14/16 Pct Recovery = 94% Analysis Date = 03/14/16 Pct Recovery = 94% Analysis Date = 03/09/16 Pct Recovery = 94% Analysis Date = 03/09/16 Pct Recovery = 94% Analysis Date = 03/04/16 Pct Recovery = 94% Analysis Date = 03/04/16 Pct Recovery = 94% Analysis Date = 02/29/16 Pct Recovery = 94% Analysis Date = 02/29/16 Pct Recovery = 94% Analysis Date = 02/24/16 Pct Recovery = 94% Analysis Date = 02/24/16 Pct Recovery = 94% Analysis Date = 02/19/16 Pct Recovery = 93% Analysis Date = 02/19/16 Pct Recovery = 93% Analysis Date = 02/14/16 Pct Recovery = 93% Analysis Date = 02/14/16 Pct Recovery = 93% Analysis Date = 02/10/16 Pct Recovery = 93% Analysis Date = 02/10/16 Pct Recovery = 93% Analysis Date = 02/05/16 Pct Recovery = 93% Analysis Date = 02/05/16 Pct Recovery = 93% Analysis Date = 01/31/16 Pct Recovery = 93% Analysis Date = 01/31/16 Pct Recovery = 93% Analysis Date = 01/26/16 Pct Recovery = 93% Analysis Date = 01/26/16 Pct Recovery = 93% Analysis Date = 01/21/16 Pct Recovery = 93% Analysis Date = 01/21/16 Pct Recovery = 93% Analysis Date = 01/17/16 Pct Recovery = 93% Analysis Date = 01/17/16 Pct Recovery = 93% Analysis Date = 01/12/16 Pct Recovery = 93% Analysis Date = 01/12/16 Pct Recovery = 93% Analysis Date = 01/07/16 Pct Recovery = 93% Analysis Date = 01/07/16 Pct Recovery = 93% Analysis Date = 01/02/16 Pct Recovery = 93% Analysis Date = 01/02/16 Pct Recovery = 93% Analysis Date = 12/29/15 Pct Recovery = 93% Analysis Date = 12/29/15 Pct Recovery = 93% Analysis Date = 12/24/15 Pct Recovery = 93% Analysis Date = 12/24/15 Pct Recovery = 93% Analysis Date = 12/19/15 Pct Recovery = 92% Analysis Date = 12/19/15 Pct Recovery = 92% Analysis Date = 12/14/15 Pct Recovery = 92% Analysis Date = 12/14/15 Pct Recovery = 92% Analysis Date = 12/09/15 Pct Recovery = 92% Analysis Date = 12/09/15 Pct Recovery = 92% Analysis Date = 12/05/15 Pct Recovery = 92% Analysis Date = 12/05/15 Pct Recovery = 92% Analysis Date = 11/30/15 Pct Recovery = 92% Analysis Date = 11/30/15 Pct Recovery = 92% Analysis Date = 11/25/15 Pct Recovery = 92% Analysis Date = 11/25/15 Pct Recovery = 92% Analysis Date = 11/20/15 Pct Recovery = 92% Analysis Date = 11/20/15 Pct Recovery = 92% Analysis Date = 11/16/15 Pct Recovery = 92% Analysis Date = 11/16/15 Pct Recovery = 92% Analysis Date = 11/11/15 Pct Recovery = 92% Analysis Date = 11/11/15 Pct Recovery = 92% Analysis Date = 11/06/15 Pct Recovery = 92% Analysis Date = 11/06/15 Pct Recovery = 92% Analysis Date = 11/01/15 Pct Recovery = 92% Analysis Date = 11/01/15 Pct Recovery = 92% Analysis Date = 10/27/15 Pct Recovery = 92% Analysis Date = 10/27/15 Pct Recovery = 92% Analysis Date = 10/23/15 Pct Recovery = 92% Analysis Date = 10/23/15 Pct Recovery = 92% Analysis Date = 10/18/15 Pct Recovery = 92% Analysis Date = 10/18/15 Pct Recovery = 92% Analysis Date = 10/13/15 Pct Recovery = 92% Analysis Date = 10/13/15 Pct Recovery = 92% Analysis Date = 10/08/15 Pct Recovery = 92% Analysis Date = 10/08/15 Pct Recovery = 92% Analysis Date = 10/04/15 Pct Recovery = 92% Analysis Date = 10/04/15 Pct Recovery = 92% Analysis Date = 09/29/15 Pct Recovery = 92% Analysis Date = 09/29/15 Pct Recovery = 92% Analysis Date = 09/24/15 Pct Recovery = 92% Analysis Date = 09/24/15 Pct Recovery = 92% Analysis Date = 09/19/15 Pct Recovery = 92% Analysis Date = 09/19/15 Pct Recovery = 92% Analysis Date = 09/14/15 Pct Recovery = 92% Analysis Date = 09/14/15 Pct Recovery = 92% Analysis Date = 09/10/15 Pct Recovery = 92% Analysis Date = 09/10/15 Pct Recovery = 92% Analysis Date = 09/05/15 Pct Recovery = 92% Analysis Date = 09/05/15 Pct Recovery = 92% Analysis Date = 08/31/15 Pct Recovery = 92% Analysis Date = 08/31/15 Pct Recovery = 92% Analysis Date = 08/26/15 Pct Recovery = 92% Analysis Date = 08/26/15 Pct Recovery = 92% Analysis Date = 08/21/15 Pct Recovery = 92% Analysis Date = 08/21/15 Pct Recovery = 92% Analysis Date = 08/17/15 Pct Recovery = 92% Analysis Date = 08/17/15 Pct Recovery = 92% Analysis Date = 08/12/15 Pct Recovery = 93% Analysis Date = 08/12/15 Pct Recovery = 93% Analysis Date = 08/07/15 Pct Recovery = 93% Analysis Date = 08/07/15 Pct Recovery = 93% Analysis Date = 08/02/15 Pct Recovery = 93% Analysis Date = 08/02/15 Pct Recovery = 93% Analysis Date = 07/29/15 Pct Recovery = 93% Analysis Date = 07/29/15 Pct Recovery = 93% Analysis Date = 07/24/15 Pct Recovery = 93% Analysis Date = 07/24/15 Pct Recovery = 93% Analysis Date = 07/19/15 Pct Recovery = 93% Analysis Date = 07/19/15 Pct Recovery = 93% Analysis Date = 07/14/15 Pct Recovery = 93% Analysis Date = 07/14/15 Pct Recovery = 93% Analysis Date = 07/09/15 Pct Recovery = 93% Analysis Date = 07/09/15 Pct Recovery = 93% Analysis Date = 07/05/15 Pct Recovery = 93% Analysis Date = 07/05/15 Pct Recovery = 93% Analysis Date = 06/30/15 Pct Recovery = 93% Analysis Date = 06/30/15 Pct Recovery = 93% Analysis Date = 06/25/15 Pct Recovery = 93% Analysis Date = 06/25/15 Pct Recovery = 93% Analysis Date = 06/20/15 Pct Recovery = 93% Analysis Date = 06/20/15 Pct Recovery = 93% Analysis Date = 06/16/15 Pct Recovery = 93% Analysis Date = 06/16/15 Pct Recovery = 93% Analysis Date = 06/11/15 Pct Recovery = 93% Analysis Date = 06/11/15 Pct Recovery = 93% Analysis Date = 06/06/15 Pct Recovery = 93% Analysis Date = 06/06/15 Pct Recovery = 93% Analysis Date = 06/01/15 Pct Recovery = 94% Analysis Date = 06/01/15 Pct Recovery = 94% Analysis Date = 05/27/15 Pct Recovery = 94% Analysis Date = 05/27/15 Pct Recovery = 94% Analysis Date = 05/23/15 Pct Recovery = 94% Analysis Date = 05/23/15 Pct Recovery = 94% Analysis Date = 05/18/15 Pct Recovery = 94% Analysis Date = 05/18/15 Pct Recovery = 94% Analysis Date = 05/13/15 Pct Recovery = 94% Analysis Date = 05/13/15 Pct Recovery = 94% Analysis Date = 05/08/15 Pct Recovery = 94% Analysis Date = 05/08/15 Pct Recovery = 94% Analysis Date = 05/04/15 Pct Recovery = 94% Analysis Date = 05/04/15 Pct Recovery = 94% Analysis Date = 04/29/15 Pct Recovery = 94% Analysis Date = 04/29/15 Pct Recovery = 94% Analysis Date = 04/24/15 Pct Recovery = 94% Analysis Date = 04/24/15 Pct Recovery = 94% Analysis Date = 04/19/15 Pct Recovery = 94% Analysis Date = 04/19/15 Pct Recovery = 94% Analysis Date = 04/14/15 Pct Recovery = 94% Analysis Date = 04/14/15 Pct Recovery = 94% Analysis Date = 04/10/15 Pct Recovery = 94% Analysis Date = 04/10/15 Pct Recovery = 94% Analysis Date = 04/05/15 Pct Recovery = 94% Analysis Date = 04/05/15 Pct Recovery = 94% Analysis Date = 03/31/15 Pct Recovery = 94% Analysis Date = 03/31/15 Pct Recovery = 94% Analysis Date = 03/26/15 Pct Recovery = 94% Analysis Date = 03/26/15 Pct Recovery = 94% Analysis Date = 03/22/15 Pct Recovery = 94% Analysis Date = 03/22/15 Pct Recovery = 94% Analysis Date = 03/17/15 Pct Recovery = 94% Analysis Date = 03/17/15 Pct Recovery = 94% Analysis Date = 03/12/15 Pct Recovery = 94% Analysis Date = 03/12/15 Pct Recovery = 94% Analysis Date = 03/07/15 Pct Recovery = 94% Analysis Date = 03/07/15 Pct Recovery = 94% Analysis Date = 03/02/15 Pct Recovery = 94% Analysis Date = 03/02/15 Pct Recovery = 94% Analysis Date = 02/26/15 Pct Recovery = 94% Analysis Date = 02/26/15 Pct Recovery = 94% Analysis Date = 02/21/15 Pct Recovery = 94% Analysis Date = 02/21/15 Pct Recovery = 94% Analysis Date = 02/16/15 Pct Recovery = 94% Analysis Date = 02/16/15 Pct Recovery = 94% Analysis Date = 02/11/15 Pct Recovery = 94% Analysis Date = 02/11/15 Pct Recovery = 94% Analysis Date = 02/07/15 Pct Recovery = 94% Analysis Date = 02/07/15 Pct Recovery = 94% Analysis Date = 02/02/15 Pct Recovery = 94% Analysis Date = 02/02/15 Pct Recovery = 94% Analysis Date = 01/28/15 Pct Recovery = 94% Analysis Date = 01/28/15 Pct Recovery = 94% Analysis Date = 01/23/15 Pct Recovery = 94% Analysis Date = 01/23/15 Pct Recovery = 94% Analysis Date = 01/18/15 Pct Recovery = 94% Analysis Date = 01/18/15 Pct Recovery = 94% Analysis Date = 01/14/15 Pct Recovery = 94% Analysis Date = 01/14/15 Pct Recovery = 94% Analysis Date = 01/09/15 Pct Recovery = 94% Analysis Date = 01/09/15 Pct Recovery = 94% Analysis Date = 01/04/15 Pct Recovery = 94% Analysis Date = 01/04/15 Pct Recovery = 94% Analysis Date = 12/30/14 Pct Recovery = 94% Analysis Date = 12/30/14 Pct Recovery = 94% Analysis Date = 12/25/14 Pct Recovery = 94% Analysis Date = 12/25/14 Pct Recovery = 94% Analysis Date = 12/21/14 Pct Recovery = 94% Analysis Date = 12/21/14 Pct Recovery = 94% Analysis Date = 12/16/14 Pct Recovery = 94% Analysis Date = 12/16/14 Pct Recovery = 94% Analysis Date = 12/11/14 Pct Recovery = 94% Analysis Date = 12/11/14 Pct Recovery = 94% Analysis Date = 12/06/14 Pct Recovery = 94% Analysis Date = 12/06/14 Pct Recovery = 94% Analysis Date = 12/02/14 Pct Recovery = 94% Analysis Date = 12/02/14 Pct Recovery = 94% Analysis Date = 11/27/14 Pct Recovery = 94% Analysis Date = 11/27/14 Pct Recovery = 94% Analysis Date = 11/22/14 Pct Recovery = 94% Analysis Date = 11/22/14 Pct Recovery = 94% Analysis Date = 11/17/14 Pct Recovery = 93% Analysis Date = 11/17/14 Pct Recovery = 93% Analysis Date = 11/12/14 Pct Recovery = 93% Analysis Date = 11/12/14 Pct Recovery = 93% Analysis Date = 11/08/14 Pct Recovery = 93% Analysis Date = 11/08/14 Pct Recovery = 93% Analysis Date = 11/03/14 Pct Recovery = 93% Analysis Date = 11/03/14 Pct Recovery = 93% Analysis Date = 10/29/14 Pct Recovery = 93% Analysis Date = 10/29/14 Pct Recovery = 93% Analysis Date = 10/24/14 Pct Recovery = 93% Analysis Date = 10/24/14 Pct Recovery = 93% Analysis Date = 10/20/14 Pct Recovery = 93% Analysis Date = 10/20/14 Pct Recovery = 93% Analysis Date = 10/15/14 Pct Recovery = 93% Analysis Date = 10/15/14 Pct Recovery = 93% Analysis Date = 10/10/14 Pct Recovery = 92% Analysis Date = 10/10/14 Pct Recovery = 92% Analysis Date = 10/05/14 Pct Recovery = 92% Analysis Date = 10/05/14 Pct Recovery = 92% Analysis Date = 09/30/14 Pct Recovery = 92% Analysis Date = 09/30/14 Pct Recovery = 92% Analysis Date = 09/26/14 Pct Recovery = 92% Analysis Date = 09/26/14 Pct Recovery = 92% Analysis Date = 09/21/14 Pct Recovery = 92% Analysis Date = 09/21/14 Pct Recovery = 92% Analysis Date = 09/16/14 Pct Recovery = 92% Analysis Date = 09/16/14 Pct Recovery = 92% Analysis Date = 09/11/14 Pct Recovery = 91% Analysis Date = 09/11/14 Pct Recovery = 91% Analysis Date = 09/07/14 Pct Recovery = 91% Analysis Date = 09/07/14 Pct Recovery = 91% Analysis Date = 09/02/14 Pct Recovery = 91% Analysis Date = 09/02/14 Pct Recovery = 91% Analysis Date = 08/28/14 Pct Recovery = 91% Analysis Date = 08/28/14 Pct Recovery = 91% Analysis Date = 08/23/14 Pct Recovery = 91% Analysis Date = 08/23/14 Pct Recovery = 91% Analysis Date = 08/18/14 Pct Recovery = 91% Analysis Date = 08/18/14 Pct Recovery = 91% Analysis Date = 08/14/14 Pct Recovery = 91% Analysis Date = 08/14/14 Pct Recovery = 91% Analysis Date = 08/09/14 Pct Recovery = 90% Analysis Date = 08/09/14 Pct Recovery = 90% Analysis Date = 08/04/14 Pct Recovery = 90% Analysis Date = 08/04/14 Pct Recovery = 90% Analysis Date = 07/30/14 Pct Recovery = 90% Analysis Date = 07/30/14 Pct Recovery = 90% Analysis Date = 07/26/14 Pct Recovery = 90% Analysis Date = 07/26/14 Pct Recovery = 90% Analysis Date = 07/21/14 Pct Recovery = 90% Analysis Date = 07/21/14 Pct Recovery = 90% Analysis Date = 07/16/14 Pct Recovery = 90% Analysis Date = 07/16/14 Pct Recovery = 90% Analysis Date = 07/11/14 Pct Recovery = 89% Analysis Date = 07/11/14 Pct Recovery = 89% Analysis Date = 07/06/14 Pct Recovery = 89% Analysis Date = 07/06/14 Pct Recovery = 89% Analysis Date = 07/02/14 Pct Recovery = 89% Analysis Date = 07/02/14 Pct Recovery = 89% Analysis Date = 06/27/14 Pct Recovery = 89% Analysis Date = 06/27/14 Pct Recovery = 89% Analysis Date = 06/22/14 Pct Recovery = 89% Analysis Date = 06/22/14 Pct Recovery = 89% Analysis Date = 06/17/14 Pct Recovery = 89% Analysis Date = 06/17/14 Pct Recovery = 89% Analysis Date = 06/13/14 Pct Recovery = 88% Analysis Date = 06/13/14 Pct Recovery = 88% Analysis Date = 06/08/14 Pct Recovery = 88% Analysis Date = 06/08/14 Pct Recovery = 88% Analysis Date = 06/03/14 Pct Recovery = 88% Analysis Date = 06/03/14 Pct Recovery = 88% Analysis Date = 05/29/14 Pct Recovery = 88% Analysis Date = 05/29/14 Pct Recovery = 88% Analysis Date = 05/24/14 Pct Recovery = 88% Analysis Date = 05/24/14 Pct Recovery = 88% Analysis Date = 05/20/14 Pct Recovery = 87% Analysis Date = 05/20/14 Pct Recovery = 87% Analysis Date = 05/15/14 Pct Recovery = 87% Analysis Date = 05/15/14 Pct Recovery = 87% Analysis Date = 05/10/14 Pct Recovery = 87% Analysis Date = 05/10/14 Pct Recovery = 87% Analysis Date = 05/05/14 Pct Recovery = 87% Analysis Date = 05/05/14 Pct Recovery = 87% Analysis Date = 05/01/14 Pct Recovery = 87% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
1,3-DICHLOROBENZENE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 43 93% 9% 96% 11%
Total 43 93% 9% 96% 11%

Sample Statistics
1,3-DICHLOROBENZENE

Characteristic N % % Basis
Plotted 43 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 43 .  
False Negatives 0 0% 0 out of 43
Not Spiked 23 .  
False Positives 0 0% 0 out of 23

BQS OBSP Determination:
1,3-DICHLOROPROPANE
METHOD: 4440 , TESTIDCODE: 77173GCM66
Open Data Set

Analysis Date = 12/12/16 SpikeMix = Accu 216041125: 40 µl & Crescent 03FF058: 40 µl Pct Recovery = 95% Analysis Date = 07/20/16 SpikeMix = Supelco LC20141V: 40 µl & Accu 216041125: 40 µl Pct Recovery = 95% Analysis Date = 07/14/16 SpikeMix = Accu 216041125: 40 µl & NSI 041816AVOC: 40 µl Pct Recovery = 90% Analysis Date = 08/12/16 SpikeMix = ChemService 5082900: 25 µl & Phenova B20160319: 25 µl Pct Recovery = 91% Analysis Date = 06/21/16 SpikeMix = Phenova B20160319: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 100% Analysis Date = 09/08/16 SpikeMix = Supelco LC20141V: 25 µl & Accu 216041125: 25 µl Pct Recovery = 85% Analysis Date = 05/24/16 SpikeMix = Accu 216041125: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 96% Analysis Date = 04/09/15 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 99% Analysis Date = 08/19/14 SpikeMix = Spex Organics C1140417015: 20 µl & Accu 214031115: 20 µl Pct Recovery = 95% Analysis Date = 07/01/14 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 94% Analysis Date = 05/01/14 SpikeMix = Accu 214031115: 20 µl & NSI 032614: 20 µl Pct Recovery = 88% Analysis Date = 03/19/15 SpikeMix = Spex Organics C1140417015: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 107% Analysis Date = 12/17/14 SpikeMix = Supelco LC06438: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 102% Analysis Date = 11/14/14 SpikeMix = Crescent 03DD004: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 92% Analysis Date = 06/10/14 SpikeMix = Crescent 03DD004: 20 µl & NSI 032614: 20 µl Pct Recovery = 87% Analysis Date = 09/29/15 SpikeMix = Accu 215041380: 25 µl & ERA 0406-15-03: 25 µl Pct Recovery = 94% Analysis Date = 08/15/15 SpikeMix = Supelco LC13545: 25 µl & Crescent 04EE008: 25 µl Pct Recovery = 97% Analysis Date = 07/13/15 SpikeMix = Crescent 04EE008: 25 µl & NSI 050515AVOC: 25 µl Pct Recovery = 98% Analysis Date = 11/29/16 SpikeMix = ChemService 5082900: 15 µl & Phenova B20160319: 15 µl Pct Recovery = 92% Analysis Date = 09/08/16 SpikeMix = Phenova B20160319: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 94% Analysis Date = 07/29/16 SpikeMix = Phenova B20160319: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 93% Analysis Date = 05/27/16 SpikeMix = Phenova B20160319: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 98% Analysis Date = 10/13/16 SpikeMix = Accu 216041125: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 89% Analysis Date = 08/20/16 SpikeMix = Accu 216041125: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 103% Analysis Date = 06/30/16 SpikeMix = ChemService 5082900: 15 µl & Accu 216041125: 15 µl Pct Recovery = 71% Analysis Date = 04/02/16 SpikeMix = Supelco LC13545: 15 µl & Accu 215041380: 15 µl Pct Recovery = 99% Analysis Date = 03/04/16 SpikeMix = Accu 215041380: 15 µl & ERA 0406-15-03: 15 µl Pct Recovery = 81% Analysis Date = 06/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Accu 215041380: 15 µl Pct Recovery = 98% Analysis Date = 12/18/15 SpikeMix = Supelco LC13545: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 90% Analysis Date = 10/17/15 SpikeMix = Crescent 04EE008: 15 µl & NSI 050515AVOC: 15 µl Pct Recovery = 102% Analysis Date = 05/09/15 SpikeMix = Spex Organics EN150428007: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 98% Analysis Date = 01/13/15 SpikeMix = Accu 214031115: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 90% Analysis Date = 09/09/14 SpikeMix = Accu 214031115: 10 µl & NSI 032614: 10 µl Pct Recovery = 101% Analysis Date = 07/23/14 SpikeMix = Spex Organics C1140417015: 10 µl & Accu 214031115: 10 µl Pct Recovery = 99% Analysis Date = 06/18/14 SpikeMix = Supelco LC06438: 10 µl & Accu 214031115: 10 µl Pct Recovery = 93% Analysis Date = 11/06/14 SpikeMix = Spex Organics C1140417015: 10 µl & Crescent 03DD004: 10 µl Pct Recovery = 99% Analysis Date = 10/04/14 SpikeMix = Crescent 03DD004: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 97% Analysis Date = 07/29/14 SpikeMix = Crescent 03DD004: 10 µl & NSI 032614: 10 µl Pct Recovery = 102% Analysis Date = 05/03/14 SpikeMix = Crescent 03DD004: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 92% Analysis Date = 02/18/16 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 89% Analysis Date = 11/20/15 SpikeMix = Accu 215041380: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 101% Analysis Date = 11/12/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 97% Analysis Date = 05/21/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 104% Analysis Date = 05/13/16 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 93% Analysis Date = 01/27/16 SpikeMix = Crescent 04EE008: 10 µl & NSI 050515AVOC: 10 µl Pct Recovery = 97% Analysis Date = 07/31/15 SpikeMix = Crescent 04EE008: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 81% Analysis Date = 05/09/15 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 102% Analysis Date = 12/11/16 Pct Recovery = 92% Analysis Date = 12/07/16 Pct Recovery = 92% Analysis Date = 12/07/16 Pct Recovery = 92% Analysis Date = 12/02/16 Pct Recovery = 92% Analysis Date = 12/02/16 Pct Recovery = 92% Analysis Date = 11/27/16 Pct Recovery = 92% Analysis Date = 11/27/16 Pct Recovery = 92% Analysis Date = 11/22/16 Pct Recovery = 92% Analysis Date = 11/22/16 Pct Recovery = 92% Analysis Date = 11/18/16 Pct Recovery = 92% Analysis Date = 11/18/16 Pct Recovery = 92% Analysis Date = 11/13/16 Pct Recovery = 92% Analysis Date = 11/13/16 Pct Recovery = 92% Analysis Date = 11/08/16 Pct Recovery = 92% Analysis Date = 11/08/16 Pct Recovery = 92% Analysis Date = 11/03/16 Pct Recovery = 92% Analysis Date = 11/03/16 Pct Recovery = 92% Analysis Date = 10/29/16 Pct Recovery = 92% Analysis Date = 10/29/16 Pct Recovery = 92% Analysis Date = 10/25/16 Pct Recovery = 92% Analysis Date = 10/25/16 Pct Recovery = 92% Analysis Date = 10/20/16 Pct Recovery = 92% Analysis Date = 10/20/16 Pct Recovery = 92% Analysis Date = 10/15/16 Pct Recovery = 92% Analysis Date = 10/15/16 Pct Recovery = 92% Analysis Date = 10/10/16 Pct Recovery = 92% Analysis Date = 10/10/16 Pct Recovery = 92% Analysis Date = 10/06/16 Pct Recovery = 92% Analysis Date = 10/06/16 Pct Recovery = 92% Analysis Date = 10/01/16 Pct Recovery = 92% Analysis Date = 10/01/16 Pct Recovery = 92% Analysis Date = 09/26/16 Pct Recovery = 92% Analysis Date = 09/26/16 Pct Recovery = 92% Analysis Date = 09/21/16 Pct Recovery = 92% Analysis Date = 09/21/16 Pct Recovery = 92% Analysis Date = 09/16/16 Pct Recovery = 92% Analysis Date = 09/16/16 Pct Recovery = 92% Analysis Date = 09/12/16 Pct Recovery = 92% Analysis Date = 09/12/16 Pct Recovery = 92% Analysis Date = 09/07/16 Pct Recovery = 92% Analysis Date = 09/07/16 Pct Recovery = 92% Analysis Date = 09/02/16 Pct Recovery = 92% Analysis Date = 09/02/16 Pct Recovery = 92% Analysis Date = 08/28/16 Pct Recovery = 92% Analysis Date = 08/28/16 Pct Recovery = 92% Analysis Date = 08/24/16 Pct Recovery = 92% Analysis Date = 08/24/16 Pct Recovery = 92% Analysis Date = 08/19/16 Pct Recovery = 92% Analysis Date = 08/19/16 Pct Recovery = 92% Analysis Date = 08/14/16 Pct Recovery = 92% Analysis Date = 08/14/16 Pct Recovery = 92% Analysis Date = 08/09/16 Pct Recovery = 92% Analysis Date = 08/09/16 Pct Recovery = 92% Analysis Date = 08/04/16 Pct Recovery = 92% Analysis Date = 08/04/16 Pct Recovery = 92% Analysis Date = 07/31/16 Pct Recovery = 92% Analysis Date = 07/31/16 Pct Recovery = 92% Analysis Date = 07/26/16 Pct Recovery = 92% Analysis Date = 07/26/16 Pct Recovery = 92% Analysis Date = 07/21/16 Pct Recovery = 92% Analysis Date = 07/21/16 Pct Recovery = 92% Analysis Date = 07/16/16 Pct Recovery = 92% Analysis Date = 07/16/16 Pct Recovery = 92% Analysis Date = 07/12/16 Pct Recovery = 92% Analysis Date = 07/12/16 Pct Recovery = 92% Analysis Date = 07/07/16 Pct Recovery = 92% Analysis Date = 07/07/16 Pct Recovery = 92% Analysis Date = 07/02/16 Pct Recovery = 92% Analysis Date = 07/02/16 Pct Recovery = 92% Analysis Date = 06/27/16 Pct Recovery = 92% Analysis Date = 06/27/16 Pct Recovery = 92% Analysis Date = 06/22/16 Pct Recovery = 92% Analysis Date = 06/22/16 Pct Recovery = 92% Analysis Date = 06/18/16 Pct Recovery = 92% Analysis Date = 06/18/16 Pct Recovery = 92% Analysis Date = 06/13/16 Pct Recovery = 92% Analysis Date = 06/13/16 Pct Recovery = 92% Analysis Date = 06/08/16 Pct Recovery = 92% Analysis Date = 06/08/16 Pct Recovery = 92% Analysis Date = 06/03/16 Pct Recovery = 93% Analysis Date = 06/03/16 Pct Recovery = 93% Analysis Date = 05/30/16 Pct Recovery = 93% Analysis Date = 05/30/16 Pct Recovery = 93% Analysis Date = 05/25/16 Pct Recovery = 93% Analysis Date = 05/25/16 Pct Recovery = 93% Analysis Date = 05/20/16 Pct Recovery = 93% Analysis Date = 05/20/16 Pct Recovery = 93% Analysis Date = 05/15/16 Pct Recovery = 93% Analysis Date = 05/15/16 Pct Recovery = 93% Analysis Date = 05/10/16 Pct Recovery = 93% Analysis Date = 05/10/16 Pct Recovery = 93% Analysis Date = 05/06/16 Pct Recovery = 93% Analysis Date = 05/06/16 Pct Recovery = 93% Analysis Date = 05/01/16 Pct Recovery = 93% Analysis Date = 05/01/16 Pct Recovery = 93% Analysis Date = 04/26/16 Pct Recovery = 93% Analysis Date = 04/26/16 Pct Recovery = 93% Analysis Date = 04/21/16 Pct Recovery = 93% Analysis Date = 04/21/16 Pct Recovery = 93% Analysis Date = 04/16/16 Pct Recovery = 93% Analysis Date = 04/16/16 Pct Recovery = 93% Analysis Date = 04/12/16 Pct Recovery = 93% Analysis Date = 04/12/16 Pct Recovery = 93% Analysis Date = 04/07/16 Pct Recovery = 93% Analysis Date = 04/07/16 Pct Recovery = 93% Analysis Date = 04/02/16 Pct Recovery = 93% Analysis Date = 04/02/16 Pct Recovery = 93% Analysis Date = 03/28/16 Pct Recovery = 93% Analysis Date = 03/28/16 Pct Recovery = 93% Analysis Date = 03/24/16 Pct Recovery = 93% Analysis Date = 03/24/16 Pct Recovery = 93% Analysis Date = 03/19/16 Pct Recovery = 93% Analysis Date = 03/19/16 Pct Recovery = 93% Analysis Date = 03/14/16 Pct Recovery = 93% Analysis Date = 03/14/16 Pct Recovery = 93% Analysis Date = 03/09/16 Pct Recovery = 93% Analysis Date = 03/09/16 Pct Recovery = 93% Analysis Date = 03/04/16 Pct Recovery = 93% Analysis Date = 03/04/16 Pct Recovery = 93% Analysis Date = 02/29/16 Pct Recovery = 93% Analysis Date = 02/29/16 Pct Recovery = 93% Analysis Date = 02/24/16 Pct Recovery = 93% Analysis Date = 02/24/16 Pct Recovery = 93% Analysis Date = 02/19/16 Pct Recovery = 94% Analysis Date = 02/19/16 Pct Recovery = 94% Analysis Date = 02/14/16 Pct Recovery = 94% Analysis Date = 02/14/16 Pct Recovery = 94% Analysis Date = 02/10/16 Pct Recovery = 94% Analysis Date = 02/10/16 Pct Recovery = 94% Analysis Date = 02/05/16 Pct Recovery = 94% Analysis Date = 02/05/16 Pct Recovery = 94% Analysis Date = 01/31/16 Pct Recovery = 94% Analysis Date = 01/31/16 Pct Recovery = 94% Analysis Date = 01/26/16 Pct Recovery = 94% Analysis Date = 01/26/16 Pct Recovery = 94% Analysis Date = 01/21/16 Pct Recovery = 94% Analysis Date = 01/21/16 Pct Recovery = 94% Analysis Date = 01/17/16 Pct Recovery = 94% Analysis Date = 01/17/16 Pct Recovery = 94% Analysis Date = 01/12/16 Pct Recovery = 94% Analysis Date = 01/12/16 Pct Recovery = 94% Analysis Date = 01/07/16 Pct Recovery = 94% Analysis Date = 01/07/16 Pct Recovery = 94% Analysis Date = 01/02/16 Pct Recovery = 94% Analysis Date = 01/02/16 Pct Recovery = 94% Analysis Date = 12/29/15 Pct Recovery = 94% Analysis Date = 12/29/15 Pct Recovery = 94% Analysis Date = 12/24/15 Pct Recovery = 94% Analysis Date = 12/24/15 Pct Recovery = 94% Analysis Date = 12/19/15 Pct Recovery = 94% Analysis Date = 12/19/15 Pct Recovery = 94% Analysis Date = 12/14/15 Pct Recovery = 94% Analysis Date = 12/14/15 Pct Recovery = 94% Analysis Date = 12/09/15 Pct Recovery = 94% Analysis Date = 12/09/15 Pct Recovery = 94% Analysis Date = 12/05/15 Pct Recovery = 94% Analysis Date = 12/05/15 Pct Recovery = 94% Analysis Date = 11/30/15 Pct Recovery = 94% Analysis Date = 11/30/15 Pct Recovery = 94% Analysis Date = 11/25/15 Pct Recovery = 95% Analysis Date = 11/25/15 Pct Recovery = 95% Analysis Date = 11/20/15 Pct Recovery = 95% Analysis Date = 11/20/15 Pct Recovery = 95% Analysis Date = 11/16/15 Pct Recovery = 95% Analysis Date = 11/16/15 Pct Recovery = 95% Analysis Date = 11/11/15 Pct Recovery = 95% Analysis Date = 11/11/15 Pct Recovery = 95% Analysis Date = 11/06/15 Pct Recovery = 95% Analysis Date = 11/06/15 Pct Recovery = 95% Analysis Date = 11/01/15 Pct Recovery = 95% Analysis Date = 11/01/15 Pct Recovery = 95% Analysis Date = 10/27/15 Pct Recovery = 95% Analysis Date = 10/27/15 Pct Recovery = 95% Analysis Date = 10/23/15 Pct Recovery = 95% Analysis Date = 10/23/15 Pct Recovery = 95% Analysis Date = 10/18/15 Pct Recovery = 95% Analysis Date = 10/18/15 Pct Recovery = 95% Analysis Date = 10/13/15 Pct Recovery = 95% Analysis Date = 10/13/15 Pct Recovery = 95% Analysis Date = 10/08/15 Pct Recovery = 96% Analysis Date = 10/08/15 Pct Recovery = 96% Analysis Date = 10/04/15 Pct Recovery = 96% Analysis Date = 10/04/15 Pct Recovery = 96% Analysis Date = 09/29/15 Pct Recovery = 96% Analysis Date = 09/29/15 Pct Recovery = 96% Analysis Date = 09/24/15 Pct Recovery = 96% Analysis Date = 09/24/15 Pct Recovery = 96% Analysis Date = 09/19/15 Pct Recovery = 96% Analysis Date = 09/19/15 Pct Recovery = 96% Analysis Date = 09/14/15 Pct Recovery = 96% Analysis Date = 09/14/15 Pct Recovery = 96% Analysis Date = 09/10/15 Pct Recovery = 96% Analysis Date = 09/10/15 Pct Recovery = 96% Analysis Date = 09/05/15 Pct Recovery = 96% Analysis Date = 09/05/15 Pct Recovery = 96% Analysis Date = 08/31/15 Pct Recovery = 96% Analysis Date = 08/31/15 Pct Recovery = 96% Analysis Date = 08/26/15 Pct Recovery = 96% Analysis Date = 08/26/15 Pct Recovery = 96% Analysis Date = 08/21/15 Pct Recovery = 96% Analysis Date = 08/21/15 Pct Recovery = 96% Analysis Date = 08/17/15 Pct Recovery = 97% Analysis Date = 08/17/15 Pct Recovery = 97% Analysis Date = 08/12/15 Pct Recovery = 97% Analysis Date = 08/12/15 Pct Recovery = 97% Analysis Date = 08/07/15 Pct Recovery = 97% Analysis Date = 08/07/15 Pct Recovery = 97% Analysis Date = 08/02/15 Pct Recovery = 97% Analysis Date = 08/02/15 Pct Recovery = 97% Analysis Date = 07/29/15 Pct Recovery = 97% Analysis Date = 07/29/15 Pct Recovery = 97% Analysis Date = 07/24/15 Pct Recovery = 97% Analysis Date = 07/24/15 Pct Recovery = 97% Analysis Date = 07/19/15 Pct Recovery = 97% Analysis Date = 07/19/15 Pct Recovery = 97% Analysis Date = 07/14/15 Pct Recovery = 97% Analysis Date = 07/14/15 Pct Recovery = 97% Analysis Date = 07/09/15 Pct Recovery = 97% Analysis Date = 07/09/15 Pct Recovery = 97% Analysis Date = 07/05/15 Pct Recovery = 97% Analysis Date = 07/05/15 Pct Recovery = 97% Analysis Date = 06/30/15 Pct Recovery = 97% Analysis Date = 06/30/15 Pct Recovery = 97% Analysis Date = 06/25/15 Pct Recovery = 97% Analysis Date = 06/25/15 Pct Recovery = 97% Analysis Date = 06/20/15 Pct Recovery = 97% Analysis Date = 06/20/15 Pct Recovery = 97% Analysis Date = 06/16/15 Pct Recovery = 97% Analysis Date = 06/16/15 Pct Recovery = 97% Analysis Date = 06/11/15 Pct Recovery = 97% Analysis Date = 06/11/15 Pct Recovery = 97% Analysis Date = 06/06/15 Pct Recovery = 97% Analysis Date = 06/06/15 Pct Recovery = 97% Analysis Date = 06/01/15 Pct Recovery = 98% Analysis Date = 06/01/15 Pct Recovery = 98% Analysis Date = 05/27/15 Pct Recovery = 98% Analysis Date = 05/27/15 Pct Recovery = 98% Analysis Date = 05/23/15 Pct Recovery = 98% Analysis Date = 05/23/15 Pct Recovery = 98% Analysis Date = 05/18/15 Pct Recovery = 98% Analysis Date = 05/18/15 Pct Recovery = 98% Analysis Date = 05/13/15 Pct Recovery = 98% Analysis Date = 05/13/15 Pct Recovery = 98% Analysis Date = 05/08/15 Pct Recovery = 98% Analysis Date = 05/08/15 Pct Recovery = 98% Analysis Date = 05/04/15 Pct Recovery = 98% Analysis Date = 05/04/15 Pct Recovery = 98% Analysis Date = 04/29/15 Pct Recovery = 98% Analysis Date = 04/29/15 Pct Recovery = 98% Analysis Date = 04/24/15 Pct Recovery = 98% Analysis Date = 04/24/15 Pct Recovery = 98% Analysis Date = 04/19/15 Pct Recovery = 98% Analysis Date = 04/19/15 Pct Recovery = 98% Analysis Date = 04/14/15 Pct Recovery = 98% Analysis Date = 04/14/15 Pct Recovery = 98% Analysis Date = 04/10/15 Pct Recovery = 98% Analysis Date = 04/10/15 Pct Recovery = 98% Analysis Date = 04/05/15 Pct Recovery = 98% Analysis Date = 04/05/15 Pct Recovery = 98% Analysis Date = 03/31/15 Pct Recovery = 98% Analysis Date = 03/31/15 Pct Recovery = 98% Analysis Date = 03/26/15 Pct Recovery = 98% Analysis Date = 03/26/15 Pct Recovery = 98% Analysis Date = 03/22/15 Pct Recovery = 98% Analysis Date = 03/22/15 Pct Recovery = 98% Analysis Date = 03/17/15 Pct Recovery = 98% Analysis Date = 03/17/15 Pct Recovery = 98% Analysis Date = 03/12/15 Pct Recovery = 98% Analysis Date = 03/12/15 Pct Recovery = 98% Analysis Date = 03/07/15 Pct Recovery = 98% Analysis Date = 03/07/15 Pct Recovery = 98% Analysis Date = 03/02/15 Pct Recovery = 98% Analysis Date = 03/02/15 Pct Recovery = 98% Analysis Date = 02/26/15 Pct Recovery = 98% Analysis Date = 02/26/15 Pct Recovery = 98% Analysis Date = 02/21/15 Pct Recovery = 98% Analysis Date = 02/21/15 Pct Recovery = 98% Analysis Date = 02/16/15 Pct Recovery = 98% Analysis Date = 02/16/15 Pct Recovery = 98% Analysis Date = 02/11/15 Pct Recovery = 98% Analysis Date = 02/11/15 Pct Recovery = 98% Analysis Date = 02/07/15 Pct Recovery = 98% Analysis Date = 02/07/15 Pct Recovery = 98% Analysis Date = 02/02/15 Pct Recovery = 97% Analysis Date = 02/02/15 Pct Recovery = 97% Analysis Date = 01/28/15 Pct Recovery = 97% Analysis Date = 01/28/15 Pct Recovery = 97% Analysis Date = 01/23/15 Pct Recovery = 97% Analysis Date = 01/23/15 Pct Recovery = 97% Analysis Date = 01/18/15 Pct Recovery = 97% Analysis Date = 01/18/15 Pct Recovery = 97% Analysis Date = 01/14/15 Pct Recovery = 97% Analysis Date = 01/14/15 Pct Recovery = 97% Analysis Date = 01/09/15 Pct Recovery = 97% Analysis Date = 01/09/15 Pct Recovery = 97% Analysis Date = 01/04/15 Pct Recovery = 97% Analysis Date = 01/04/15 Pct Recovery = 97% Analysis Date = 12/30/14 Pct Recovery = 97% Analysis Date = 12/30/14 Pct Recovery = 97% Analysis Date = 12/25/14 Pct Recovery = 97% Analysis Date = 12/25/14 Pct Recovery = 97% Analysis Date = 12/21/14 Pct Recovery = 97% Analysis Date = 12/21/14 Pct Recovery = 97% Analysis Date = 12/16/14 Pct Recovery = 97% Analysis Date = 12/16/14 Pct Recovery = 97% Analysis Date = 12/11/14 Pct Recovery = 97% Analysis Date = 12/11/14 Pct Recovery = 97% Analysis Date = 12/06/14 Pct Recovery = 97% Analysis Date = 12/06/14 Pct Recovery = 97% Analysis Date = 12/02/14 Pct Recovery = 97% Analysis Date = 12/02/14 Pct Recovery = 97% Analysis Date = 11/27/14 Pct Recovery = 97% Analysis Date = 11/27/14 Pct Recovery = 97% Analysis Date = 11/22/14 Pct Recovery = 97% Analysis Date = 11/22/14 Pct Recovery = 97% Analysis Date = 11/17/14 Pct Recovery = 97% Analysis Date = 11/17/14 Pct Recovery = 97% Analysis Date = 11/12/14 Pct Recovery = 97% Analysis Date = 11/12/14 Pct Recovery = 97% Analysis Date = 11/08/14 Pct Recovery = 97% Analysis Date = 11/08/14 Pct Recovery = 97% Analysis Date = 11/03/14 Pct Recovery = 97% Analysis Date = 11/03/14 Pct Recovery = 97% Analysis Date = 10/29/14 Pct Recovery = 96% Analysis Date = 10/29/14 Pct Recovery = 96% Analysis Date = 10/24/14 Pct Recovery = 96% Analysis Date = 10/24/14 Pct Recovery = 96% Analysis Date = 10/20/14 Pct Recovery = 96% Analysis Date = 10/20/14 Pct Recovery = 96% Analysis Date = 10/15/14 Pct Recovery = 96% Analysis Date = 10/15/14 Pct Recovery = 96% Analysis Date = 10/10/14 Pct Recovery = 96% Analysis Date = 10/10/14 Pct Recovery = 96% Analysis Date = 10/05/14 Pct Recovery = 96% Analysis Date = 10/05/14 Pct Recovery = 96% Analysis Date = 09/30/14 Pct Recovery = 96% Analysis Date = 09/30/14 Pct Recovery = 96% Analysis Date = 09/26/14 Pct Recovery = 96% Analysis Date = 09/26/14 Pct Recovery = 96% Analysis Date = 09/21/14 Pct Recovery = 96% Analysis Date = 09/21/14 Pct Recovery = 96% Analysis Date = 09/16/14 Pct Recovery = 96% Analysis Date = 09/16/14 Pct Recovery = 96% Analysis Date = 09/11/14 Pct Recovery = 96% Analysis Date = 09/11/14 Pct Recovery = 96% Analysis Date = 09/07/14 Pct Recovery = 96% Analysis Date = 09/07/14 Pct Recovery = 96% Analysis Date = 09/02/14 Pct Recovery = 95% Analysis Date = 09/02/14 Pct Recovery = 95% Analysis Date = 08/28/14 Pct Recovery = 95% Analysis Date = 08/28/14 Pct Recovery = 95% Analysis Date = 08/23/14 Pct Recovery = 95% Analysis Date = 08/23/14 Pct Recovery = 95% Analysis Date = 08/18/14 Pct Recovery = 95% Analysis Date = 08/18/14 Pct Recovery = 95% Analysis Date = 08/14/14 Pct Recovery = 95% Analysis Date = 08/14/14 Pct Recovery = 95% Analysis Date = 08/09/14 Pct Recovery = 95% Analysis Date = 08/09/14 Pct Recovery = 95% Analysis Date = 08/04/14 Pct Recovery = 95% Analysis Date = 08/04/14 Pct Recovery = 95% Analysis Date = 07/30/14 Pct Recovery = 95% Analysis Date = 07/30/14 Pct Recovery = 95% Analysis Date = 07/26/14 Pct Recovery = 95% Analysis Date = 07/26/14 Pct Recovery = 95% Analysis Date = 07/21/14 Pct Recovery = 95% Analysis Date = 07/21/14 Pct Recovery = 95% Analysis Date = 07/16/14 Pct Recovery = 95% Analysis Date = 07/16/14 Pct Recovery = 95% Analysis Date = 07/11/14 Pct Recovery = 94% Analysis Date = 07/11/14 Pct Recovery = 94% Analysis Date = 07/06/14 Pct Recovery = 94% Analysis Date = 07/06/14 Pct Recovery = 94% Analysis Date = 07/02/14 Pct Recovery = 94% Analysis Date = 07/02/14 Pct Recovery = 94% Analysis Date = 06/27/14 Pct Recovery = 94% Analysis Date = 06/27/14 Pct Recovery = 94% Analysis Date = 06/22/14 Pct Recovery = 94% Analysis Date = 06/22/14 Pct Recovery = 94% Analysis Date = 06/17/14 Pct Recovery = 94% Analysis Date = 06/17/14 Pct Recovery = 94% Analysis Date = 06/13/14 Pct Recovery = 94% Analysis Date = 06/13/14 Pct Recovery = 94% Analysis Date = 06/08/14 Pct Recovery = 94% Analysis Date = 06/08/14 Pct Recovery = 94% Analysis Date = 06/03/14 Pct Recovery = 94% Analysis Date = 06/03/14 Pct Recovery = 94% Analysis Date = 05/29/14 Pct Recovery = 94% Analysis Date = 05/29/14 Pct Recovery = 94% Analysis Date = 05/24/14 Pct Recovery = 94% Analysis Date = 05/24/14 Pct Recovery = 94% Analysis Date = 05/20/14 Pct Recovery = 93% Analysis Date = 05/20/14 Pct Recovery = 93% Analysis Date = 05/15/14 Pct Recovery = 93% Analysis Date = 05/15/14 Pct Recovery = 93% Analysis Date = 05/10/14 Pct Recovery = 93% Analysis Date = 05/10/14 Pct Recovery = 93% Analysis Date = 05/05/14 Pct Recovery = 93% Analysis Date = 05/05/14 Pct Recovery = 93% Analysis Date = 05/01/14 Pct Recovery = 93% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
1,3-DICHLOROPROPANE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 47 95% 7% 95% 6%
Total 47 95% 7% 95% 6%

Sample Statistics
1,3-DICHLOROPROPANE

Characteristic N % % Basis
Plotted 47 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 47 .  
False Negatives 0 0% 0 out of 47
Not Spiked 26 .  
False Positives 0 0% 0 out of 26

BQS OBSP Determination:
1,4-DICHLOROBENZENE
METHOD: 4440 , TESTIDCODE: 34571GCM66
Open Data Set

Analysis Date = 12/16/16 SpikeMix = NSI 041816AVOC: 40 µl & ChemService 5082900: 40 µl Pct Recovery = 101% Analysis Date = 08/04/16 SpikeMix = Crescent 03FF058: 40 µl & Supelco LC20141V: 40 µl Pct Recovery = 87% Analysis Date = 07/20/16 SpikeMix = Supelco LC20141V: 40 µl & Accu 216041125: 40 µl Pct Recovery = 93% Analysis Date = 11/21/16 SpikeMix = Crescent 03FF058: 25 µl & Supelco LC20141V: 25 µl Pct Recovery = 93% Analysis Date = 09/08/16 SpikeMix = Supelco LC20141V: 25 µl & Accu 216041125: 25 µl Pct Recovery = 93% Analysis Date = 08/26/16 SpikeMix = NSI 041816AVOC: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 93% Analysis Date = 08/12/16 SpikeMix = ChemService 5082900: 25 µl & Phenova B20160319: 25 µl Pct Recovery = 101% Analysis Date = 06/30/16 SpikeMix = Crescent 03FF058: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 94% Analysis Date = 04/09/15 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 90% Analysis Date = 03/06/15 SpikeMix = ERA 0227-14-06.1A: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 100% Analysis Date = 11/14/14 SpikeMix = Crescent 03DD004: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 91% Analysis Date = 08/16/14 SpikeMix = ERA 0227-14-06.1A: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 90% Analysis Date = 07/01/14 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 90% Analysis Date = 11/22/14 SpikeMix = NSI 032614: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 104% Analysis Date = 06/10/14 SpikeMix = Crescent 03DD004: 20 µl & NSI 032614: 20 µl Pct Recovery = 90% Analysis Date = 06/10/14 SpikeMix = NSI 032614: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 104% Analysis Date = 05/01/14 SpikeMix = Accu 214031115: 20 µl & NSI 032614: 20 µl Pct Recovery = 78% Analysis Date = 08/15/15 SpikeMix = Supelco LC13545: 25 µl & Crescent 04EE008: 25 µl Pct Recovery = 106% Analysis Date = 07/13/15 SpikeMix = Crescent 04EE008: 25 µl & NSI 050515AVOC: 25 µl Pct Recovery = 79% Analysis Date = 09/29/15 SpikeMix = Accu 215041380: 25 µl & ERA 0406-15-03: 25 µl Pct Recovery = 78% Analysis Date = 11/29/16 SpikeMix = ChemService 5082900: 15 µl & Phenova B20160319: 15 µl Pct Recovery = 99% Analysis Date = 10/13/16 SpikeMix = NSI 041816AVOC: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 78% Analysis Date = 09/28/16 SpikeMix = Crescent 03FF058: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 85% Analysis Date = 06/30/16 SpikeMix = ChemService 5082900: 15 µl & Accu 216041125: 15 µl Pct Recovery = 96% Analysis Date = 06/10/16 SpikeMix = NSI 041816AVOC: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 98% Analysis Date = 05/27/16 SpikeMix = Phenova B20160319: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 95% Analysis Date = 12/18/15 SpikeMix = Supelco LC13545: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 104% Analysis Date = 10/17/15 SpikeMix = Crescent 04EE008: 15 µl & NSI 050515AVOC: 15 µl Pct Recovery = 93% Analysis Date = 05/09/15 SpikeMix = Spex Organics EN150428007: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 101% Analysis Date = 04/02/16 SpikeMix = Supelco LC13545: 15 µl & Accu 215041380: 15 µl Pct Recovery = 93% Analysis Date = 03/04/16 SpikeMix = Accu 215041380: 15 µl & ERA 0406-15-03: 15 µl Pct Recovery = 87% Analysis Date = 06/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Accu 215041380: 15 µl Pct Recovery = 86% Analysis Date = 01/13/15 SpikeMix = Accu 214031115: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 80% Analysis Date = 10/21/14 SpikeMix = ERA 0227-14-06.1A: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 98% Analysis Date = 10/04/14 SpikeMix = Crescent 03DD004: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 95% Analysis Date = 07/11/14 SpikeMix = Spex Organics C1140417015: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 84% Analysis Date = 09/09/14 SpikeMix = Accu 214031115: 10 µl & NSI 032614: 10 µl Pct Recovery = 99% Analysis Date = 09/09/14 SpikeMix = NSI 032614: 10 µl & Spex Organics C1140417015: 10 µl Pct Recovery = 109% Analysis Date = 07/29/14 SpikeMix = Crescent 03DD004: 10 µl & NSI 032614: 10 µl Pct Recovery = 97% Analysis Date = 05/30/14 SpikeMix = NSI 032614: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 75% Analysis Date = 05/13/16 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 108% Analysis Date = 01/27/16 SpikeMix = Crescent 04EE008: 10 µl & NSI 050515AVOC: 10 µl Pct Recovery = 101% Analysis Date = 07/31/15 SpikeMix = Crescent 04EE008: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 95% Analysis Date = 05/09/15 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 99% Analysis Date = 02/18/16 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 94% Analysis Date = 11/20/15 SpikeMix = Accu 215041380: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 96% Analysis Date = 11/12/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 95% Analysis Date = 05/21/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 105% Analysis Date = 12/15/16 Pct Recovery = 93% Analysis Date = 12/11/16 Pct Recovery = 93% Analysis Date = 12/11/16 Pct Recovery = 93% Analysis Date = 12/06/16 Pct Recovery = 93% Analysis Date = 12/06/16 Pct Recovery = 93% Analysis Date = 12/01/16 Pct Recovery = 93% Analysis Date = 12/01/16 Pct Recovery = 93% Analysis Date = 11/26/16 Pct Recovery = 93% Analysis Date = 11/26/16 Pct Recovery = 93% Analysis Date = 11/21/16 Pct Recovery = 93% Analysis Date = 11/21/16 Pct Recovery = 93% Analysis Date = 11/17/16 Pct Recovery = 93% Analysis Date = 11/17/16 Pct Recovery = 93% Analysis Date = 11/12/16 Pct Recovery = 93% Analysis Date = 11/12/16 Pct Recovery = 93% Analysis Date = 11/07/16 Pct Recovery = 93% Analysis Date = 11/07/16 Pct Recovery = 93% Analysis Date = 11/02/16 Pct Recovery = 93% Analysis Date = 11/02/16 Pct Recovery = 93% Analysis Date = 10/28/16 Pct Recovery = 93% Analysis Date = 10/28/16 Pct Recovery = 93% Analysis Date = 10/24/16 Pct Recovery = 93% Analysis Date = 10/24/16 Pct Recovery = 93% Analysis Date = 10/19/16 Pct Recovery = 93% Analysis Date = 10/19/16 Pct Recovery = 93% Analysis Date = 10/14/16 Pct Recovery = 93% Analysis Date = 10/14/16 Pct Recovery = 93% Analysis Date = 10/09/16 Pct Recovery = 93% Analysis Date = 10/09/16 Pct Recovery = 93% Analysis Date = 10/04/16 Pct Recovery = 93% Analysis Date = 10/04/16 Pct Recovery = 93% Analysis Date = 09/30/16 Pct Recovery = 93% Analysis Date = 09/30/16 Pct Recovery = 93% Analysis Date = 09/25/16 Pct Recovery = 93% Analysis Date = 09/25/16 Pct Recovery = 93% Analysis Date = 09/20/16 Pct Recovery = 93% Analysis Date = 09/20/16 Pct Recovery = 93% Analysis Date = 09/15/16 Pct Recovery = 93% Analysis Date = 09/15/16 Pct Recovery = 93% Analysis Date = 09/10/16 Pct Recovery = 93% Analysis Date = 09/10/16 Pct Recovery = 93% Analysis Date = 09/06/16 Pct Recovery = 94% Analysis Date = 09/06/16 Pct Recovery = 94% Analysis Date = 09/01/16 Pct Recovery = 94% Analysis Date = 09/01/16 Pct Recovery = 94% Analysis Date = 08/27/16 Pct Recovery = 94% Analysis Date = 08/27/16 Pct Recovery = 94% Analysis Date = 08/22/16 Pct Recovery = 94% Analysis Date = 08/22/16 Pct Recovery = 94% Analysis Date = 08/17/16 Pct Recovery = 94% Analysis Date = 08/17/16 Pct Recovery = 94% Analysis Date = 08/13/16 Pct Recovery = 94% Analysis Date = 08/13/16 Pct Recovery = 94% Analysis Date = 08/08/16 Pct Recovery = 94% Analysis Date = 08/08/16 Pct Recovery = 94% Analysis Date = 08/03/16 Pct Recovery = 94% Analysis Date = 08/03/16 Pct Recovery = 94% Analysis Date = 07/29/16 Pct Recovery = 94% Analysis Date = 07/29/16 Pct Recovery = 94% Analysis Date = 07/24/16 Pct Recovery = 94% Analysis Date = 07/24/16 Pct Recovery = 94% Analysis Date = 07/20/16 Pct Recovery = 94% Analysis Date = 07/20/16 Pct Recovery = 94% Analysis Date = 07/15/16 Pct Recovery = 94% Analysis Date = 07/15/16 Pct Recovery = 94% Analysis Date = 07/10/16 Pct Recovery = 94% Analysis Date = 07/10/16 Pct Recovery = 94% Analysis Date = 07/05/16 Pct Recovery = 94% Analysis Date = 07/05/16 Pct Recovery = 94% Analysis Date = 06/30/16 Pct Recovery = 94% Analysis Date = 06/30/16 Pct Recovery = 94% Analysis Date = 06/26/16 Pct Recovery = 94% Analysis Date = 06/26/16 Pct Recovery = 94% Analysis Date = 06/21/16 Pct Recovery = 94% Analysis Date = 06/21/16 Pct Recovery = 94% Analysis Date = 06/16/16 Pct Recovery = 94% Analysis Date = 06/16/16 Pct Recovery = 94% Analysis Date = 06/11/16 Pct Recovery = 94% Analysis Date = 06/11/16 Pct Recovery = 94% Analysis Date = 06/06/16 Pct Recovery = 94% Analysis Date = 06/06/16 Pct Recovery = 94% Analysis Date = 06/02/16 Pct Recovery = 94% Analysis Date = 06/02/16 Pct Recovery = 94% Analysis Date = 05/28/16 Pct Recovery = 94% Analysis Date = 05/28/16 Pct Recovery = 94% Analysis Date = 05/23/16 Pct Recovery = 94% Analysis Date = 05/23/16 Pct Recovery = 94% Analysis Date = 05/18/16 Pct Recovery = 94% Analysis Date = 05/18/16 Pct Recovery = 94% Analysis Date = 05/13/16 Pct Recovery = 94% Analysis Date = 05/13/16 Pct Recovery = 94% Analysis Date = 05/09/16 Pct Recovery = 94% Analysis Date = 05/09/16 Pct Recovery = 94% Analysis Date = 05/04/16 Pct Recovery = 94% Analysis Date = 05/04/16 Pct Recovery = 94% Analysis Date = 04/29/16 Pct Recovery = 95% Analysis Date = 04/29/16 Pct Recovery = 95% Analysis Date = 04/24/16 Pct Recovery = 95% Analysis Date = 04/24/16 Pct Recovery = 95% Analysis Date = 04/19/16 Pct Recovery = 95% Analysis Date = 04/19/16 Pct Recovery = 95% Analysis Date = 04/15/16 Pct Recovery = 95% Analysis Date = 04/15/16 Pct Recovery = 95% Analysis Date = 04/10/16 Pct Recovery = 95% Analysis Date = 04/10/16 Pct Recovery = 95% Analysis Date = 04/05/16 Pct Recovery = 95% Analysis Date = 04/05/16 Pct Recovery = 95% Analysis Date = 03/31/16 Pct Recovery = 95% Analysis Date = 03/31/16 Pct Recovery = 95% Analysis Date = 03/26/16 Pct Recovery = 95% Analysis Date = 03/26/16 Pct Recovery = 95% Analysis Date = 03/22/16 Pct Recovery = 95% Analysis Date = 03/22/16 Pct Recovery = 95% Analysis Date = 03/17/16 Pct Recovery = 95% Analysis Date = 03/17/16 Pct Recovery = 95% Analysis Date = 03/12/16 Pct Recovery = 95% Analysis Date = 03/12/16 Pct Recovery = 95% Analysis Date = 03/07/16 Pct Recovery = 95% Analysis Date = 03/07/16 Pct Recovery = 95% Analysis Date = 03/02/16 Pct Recovery = 95% Analysis Date = 03/02/16 Pct Recovery = 95% Analysis Date = 02/27/16 Pct Recovery = 95% Analysis Date = 02/27/16 Pct Recovery = 95% Analysis Date = 02/22/16 Pct Recovery = 95% Analysis Date = 02/22/16 Pct Recovery = 95% Analysis Date = 02/17/16 Pct Recovery = 95% Analysis Date = 02/17/16 Pct Recovery = 95% Analysis Date = 02/12/16 Pct Recovery = 95% Analysis Date = 02/12/16 Pct Recovery = 95% Analysis Date = 02/07/16 Pct Recovery = 95% Analysis Date = 02/07/16 Pct Recovery = 95% Analysis Date = 02/03/16 Pct Recovery = 95% Analysis Date = 02/03/16 Pct Recovery = 95% Analysis Date = 01/29/16 Pct Recovery = 95% Analysis Date = 01/29/16 Pct Recovery = 95% Analysis Date = 01/24/16 Pct Recovery = 95% Analysis Date = 01/24/16 Pct Recovery = 95% Analysis Date = 01/19/16 Pct Recovery = 95% Analysis Date = 01/19/16 Pct Recovery = 95% Analysis Date = 01/14/16 Pct Recovery = 95% Analysis Date = 01/14/16 Pct Recovery = 95% Analysis Date = 01/10/16 Pct Recovery = 95% Analysis Date = 01/10/16 Pct Recovery = 95% Analysis Date = 01/05/16 Pct Recovery = 95% Analysis Date = 01/05/16 Pct Recovery = 95% Analysis Date = 12/31/15 Pct Recovery = 95% Analysis Date = 12/31/15 Pct Recovery = 95% Analysis Date = 12/26/15 Pct Recovery = 95% Analysis Date = 12/26/15 Pct Recovery = 95% Analysis Date = 12/21/15 Pct Recovery = 95% Analysis Date = 12/21/15 Pct Recovery = 95% Analysis Date = 12/17/15 Pct Recovery = 95% Analysis Date = 12/17/15 Pct Recovery = 95% Analysis Date = 12/12/15 Pct Recovery = 95% Analysis Date = 12/12/15 Pct Recovery = 95% Analysis Date = 12/07/15 Pct Recovery = 95% Analysis Date = 12/07/15 Pct Recovery = 95% Analysis Date = 12/02/15 Pct Recovery = 95% Analysis Date = 12/02/15 Pct Recovery = 95% Analysis Date = 11/27/15 Pct Recovery = 95% Analysis Date = 11/27/15 Pct Recovery = 95% Analysis Date = 11/23/15 Pct Recovery = 95% Analysis Date = 11/23/15 Pct Recovery = 95% Analysis Date = 11/18/15 Pct Recovery = 95% Analysis Date = 11/18/15 Pct Recovery = 95% Analysis Date = 11/13/15 Pct Recovery = 95% Analysis Date = 11/13/15 Pct Recovery = 95% Analysis Date = 11/08/15 Pct Recovery = 95% Analysis Date = 11/08/15 Pct Recovery = 95% Analysis Date = 11/03/15 Pct Recovery = 95% Analysis Date = 11/03/15 Pct Recovery = 95% Analysis Date = 10/30/15 Pct Recovery = 95% Analysis Date = 10/30/15 Pct Recovery = 95% Analysis Date = 10/25/15 Pct Recovery = 95% Analysis Date = 10/25/15 Pct Recovery = 95% Analysis Date = 10/20/15 Pct Recovery = 95% Analysis Date = 10/20/15 Pct Recovery = 95% Analysis Date = 10/15/15 Pct Recovery = 95% Analysis Date = 10/15/15 Pct Recovery = 95% Analysis Date = 10/10/15 Pct Recovery = 94% Analysis Date = 10/10/15 Pct Recovery = 94% Analysis Date = 10/06/15 Pct Recovery = 94% Analysis Date = 10/06/15 Pct Recovery = 94% Analysis Date = 10/01/15 Pct Recovery = 94% Analysis Date = 10/01/15 Pct Recovery = 94% Analysis Date = 09/26/15 Pct Recovery = 94% Analysis Date = 09/26/15 Pct Recovery = 94% Analysis Date = 09/21/15 Pct Recovery = 94% Analysis Date = 09/21/15 Pct Recovery = 94% Analysis Date = 09/16/15 Pct Recovery = 94% Analysis Date = 09/16/15 Pct Recovery = 94% Analysis Date = 09/12/15 Pct Recovery = 94% Analysis Date = 09/12/15 Pct Recovery = 94% Analysis Date = 09/07/15 Pct Recovery = 94% Analysis Date = 09/07/15 Pct Recovery = 94% Analysis Date = 09/02/15 Pct Recovery = 94% Analysis Date = 09/02/15 Pct Recovery = 94% Analysis Date = 08/28/15 Pct Recovery = 94% Analysis Date = 08/28/15 Pct Recovery = 94% Analysis Date = 08/23/15 Pct Recovery = 94% Analysis Date = 08/23/15 Pct Recovery = 94% Analysis Date = 08/19/15 Pct Recovery = 94% Analysis Date = 08/19/15 Pct Recovery = 94% Analysis Date = 08/14/15 Pct Recovery = 94% Analysis Date = 08/14/15 Pct Recovery = 94% Analysis Date = 08/09/15 Pct Recovery = 94% Analysis Date = 08/09/15 Pct Recovery = 94% Analysis Date = 08/04/15 Pct Recovery = 94% Analysis Date = 08/04/15 Pct Recovery = 94% Analysis Date = 07/30/15 Pct Recovery = 94% Analysis Date = 07/30/15 Pct Recovery = 94% Analysis Date = 07/26/15 Pct Recovery = 94% Analysis Date = 07/26/15 Pct Recovery = 94% Analysis Date = 07/21/15 Pct Recovery = 94% Analysis Date = 07/21/15 Pct Recovery = 94% Analysis Date = 07/16/15 Pct Recovery = 94% Analysis Date = 07/16/15 Pct Recovery = 94% Analysis Date = 07/11/15 Pct Recovery = 94% Analysis Date = 07/11/15 Pct Recovery = 94% Analysis Date = 07/06/15 Pct Recovery = 94% Analysis Date = 07/06/15 Pct Recovery = 94% Analysis Date = 07/02/15 Pct Recovery = 94% Analysis Date = 07/02/15 Pct Recovery = 94% Analysis Date = 06/27/15 Pct Recovery = 94% Analysis Date = 06/27/15 Pct Recovery = 94% Analysis Date = 06/22/15 Pct Recovery = 94% Analysis Date = 06/22/15 Pct Recovery = 94% Analysis Date = 06/17/15 Pct Recovery = 94% Analysis Date = 06/17/15 Pct Recovery = 94% Analysis Date = 06/12/15 Pct Recovery = 94% Analysis Date = 06/12/15 Pct Recovery = 94% Analysis Date = 06/08/15 Pct Recovery = 94% Analysis Date = 06/08/15 Pct Recovery = 94% Analysis Date = 06/03/15 Pct Recovery = 94% Analysis Date = 06/03/15 Pct Recovery = 94% Analysis Date = 05/29/15 Pct Recovery = 94% Analysis Date = 05/29/15 Pct Recovery = 94% Analysis Date = 05/24/15 Pct Recovery = 94% Analysis Date = 05/24/15 Pct Recovery = 94% Analysis Date = 05/19/15 Pct Recovery = 94% Analysis Date = 05/19/15 Pct Recovery = 94% Analysis Date = 05/15/15 Pct Recovery = 94% Analysis Date = 05/15/15 Pct Recovery = 94% Analysis Date = 05/10/15 Pct Recovery = 94% Analysis Date = 05/10/15 Pct Recovery = 94% Analysis Date = 05/05/15 Pct Recovery = 94% Analysis Date = 05/05/15 Pct Recovery = 94% Analysis Date = 04/30/15 Pct Recovery = 94% Analysis Date = 04/30/15 Pct Recovery = 94% Analysis Date = 04/25/15 Pct Recovery = 94% Analysis Date = 04/25/15 Pct Recovery = 94% Analysis Date = 04/21/15 Pct Recovery = 94% Analysis Date = 04/21/15 Pct Recovery = 94% Analysis Date = 04/16/15 Pct Recovery = 94% Analysis Date = 04/16/15 Pct Recovery = 94% Analysis Date = 04/11/15 Pct Recovery = 94% Analysis Date = 04/11/15 Pct Recovery = 94% Analysis Date = 04/06/15 Pct Recovery = 94% Analysis Date = 04/06/15 Pct Recovery = 94% Analysis Date = 04/01/15 Pct Recovery = 94% Analysis Date = 04/01/15 Pct Recovery = 94% Analysis Date = 03/28/15 Pct Recovery = 94% Analysis Date = 03/28/15 Pct Recovery = 94% Analysis Date = 03/23/15 Pct Recovery = 94% Analysis Date = 03/23/15 Pct Recovery = 94% Analysis Date = 03/18/15 Pct Recovery = 94% Analysis Date = 03/18/15 Pct Recovery = 94% Analysis Date = 03/13/15 Pct Recovery = 95% Analysis Date = 03/13/15 Pct Recovery = 95% Analysis Date = 03/08/15 Pct Recovery = 95% Analysis Date = 03/08/15 Pct Recovery = 95% Analysis Date = 03/04/15 Pct Recovery = 95% Analysis Date = 03/04/15 Pct Recovery = 95% Analysis Date = 02/27/15 Pct Recovery = 95% Analysis Date = 02/27/15 Pct Recovery = 95% Analysis Date = 02/22/15 Pct Recovery = 95% Analysis Date = 02/22/15 Pct Recovery = 95% Analysis Date = 02/17/15 Pct Recovery = 95% Analysis Date = 02/17/15 Pct Recovery = 95% Analysis Date = 02/12/15 Pct Recovery = 95% Analysis Date = 02/12/15 Pct Recovery = 95% Analysis Date = 02/08/15 Pct Recovery = 95% Analysis Date = 02/08/15 Pct Recovery = 95% Analysis Date = 02/03/15 Pct Recovery = 95% Analysis Date = 02/03/15 Pct Recovery = 95% Analysis Date = 01/29/15 Pct Recovery = 95% Analysis Date = 01/29/15 Pct Recovery = 95% Analysis Date = 01/24/15 Pct Recovery = 95% Analysis Date = 01/24/15 Pct Recovery = 95% Analysis Date = 01/19/15 Pct Recovery = 95% Analysis Date = 01/19/15 Pct Recovery = 95% Analysis Date = 01/15/15 Pct Recovery = 95% Analysis Date = 01/15/15 Pct Recovery = 95% Analysis Date = 01/10/15 Pct Recovery = 95% Analysis Date = 01/10/15 Pct Recovery = 95% Analysis Date = 01/05/15 Pct Recovery = 95% Analysis Date = 01/05/15 Pct Recovery = 95% Analysis Date = 12/31/14 Pct Recovery = 95% Analysis Date = 12/31/14 Pct Recovery = 95% Analysis Date = 12/26/14 Pct Recovery = 95% Analysis Date = 12/26/14 Pct Recovery = 95% Analysis Date = 12/22/14 Pct Recovery = 94% Analysis Date = 12/22/14 Pct Recovery = 94% Analysis Date = 12/17/14 Pct Recovery = 94% Analysis Date = 12/17/14 Pct Recovery = 94% Analysis Date = 12/12/14 Pct Recovery = 94% Analysis Date = 12/12/14 Pct Recovery = 94% Analysis Date = 12/07/14 Pct Recovery = 94% Analysis Date = 12/07/14 Pct Recovery = 94% Analysis Date = 12/02/14 Pct Recovery = 94% Analysis Date = 12/02/14 Pct Recovery = 94% Analysis Date = 11/28/14 Pct Recovery = 94% Analysis Date = 11/28/14 Pct Recovery = 94% Analysis Date = 11/23/14 Pct Recovery = 94% Analysis Date = 11/23/14 Pct Recovery = 94% Analysis Date = 11/18/14 Pct Recovery = 94% Analysis Date = 11/18/14 Pct Recovery = 94% Analysis Date = 11/13/14 Pct Recovery = 94% Analysis Date = 11/13/14 Pct Recovery = 94% Analysis Date = 11/08/14 Pct Recovery = 94% Analysis Date = 11/08/14 Pct Recovery = 94% Analysis Date = 11/04/14 Pct Recovery = 94% Analysis Date = 11/04/14 Pct Recovery = 94% Analysis Date = 10/30/14 Pct Recovery = 93% Analysis Date = 10/30/14 Pct Recovery = 93% Analysis Date = 10/25/14 Pct Recovery = 93% Analysis Date = 10/25/14 Pct Recovery = 93% Analysis Date = 10/20/14 Pct Recovery = 93% Analysis Date = 10/20/14 Pct Recovery = 93% Analysis Date = 10/15/14 Pct Recovery = 93% Analysis Date = 10/15/14 Pct Recovery = 93% Analysis Date = 10/11/14 Pct Recovery = 93% Analysis Date = 10/11/14 Pct Recovery = 93% Analysis Date = 10/06/14 Pct Recovery = 93% Analysis Date = 10/06/14 Pct Recovery = 93% Analysis Date = 10/01/14 Pct Recovery = 93% Analysis Date = 10/01/14 Pct Recovery = 93% Analysis Date = 09/26/14 Pct Recovery = 93% Analysis Date = 09/26/14 Pct Recovery = 93% Analysis Date = 09/21/14 Pct Recovery = 93% Analysis Date = 09/21/14 Pct Recovery = 93% Analysis Date = 09/17/14 Pct Recovery = 93% Analysis Date = 09/17/14 Pct Recovery = 93% Analysis Date = 09/12/14 Pct Recovery = 93% Analysis Date = 09/12/14 Pct Recovery = 93% Analysis Date = 09/07/14 Pct Recovery = 92% Analysis Date = 09/07/14 Pct Recovery = 92% Analysis Date = 09/02/14 Pct Recovery = 92% Analysis Date = 09/02/14 Pct Recovery = 92% Analysis Date = 08/28/14 Pct Recovery = 92% Analysis Date = 08/28/14 Pct Recovery = 92% Analysis Date = 08/24/14 Pct Recovery = 92% Analysis Date = 08/24/14 Pct Recovery = 92% Analysis Date = 08/19/14 Pct Recovery = 92% Analysis Date = 08/19/14 Pct Recovery = 92% Analysis Date = 08/14/14 Pct Recovery = 92% Analysis Date = 08/14/14 Pct Recovery = 92% Analysis Date = 08/09/14 Pct Recovery = 92% Analysis Date = 08/09/14 Pct Recovery = 92% Analysis Date = 08/04/14 Pct Recovery = 92% Analysis Date = 08/04/14 Pct Recovery = 92% Analysis Date = 07/31/14 Pct Recovery = 92% Analysis Date = 07/31/14 Pct Recovery = 92% Analysis Date = 07/26/14 Pct Recovery = 92% Analysis Date = 07/26/14 Pct Recovery = 92% Analysis Date = 07/21/14 Pct Recovery = 91% Analysis Date = 07/21/14 Pct Recovery = 91% Analysis Date = 07/16/14 Pct Recovery = 91% Analysis Date = 07/16/14 Pct Recovery = 91% Analysis Date = 07/11/14 Pct Recovery = 91% Analysis Date = 07/11/14 Pct Recovery = 91% Analysis Date = 07/07/14 Pct Recovery = 91% Analysis Date = 07/07/14 Pct Recovery = 91% Analysis Date = 07/02/14 Pct Recovery = 91% Analysis Date = 07/02/14 Pct Recovery = 91% Analysis Date = 06/27/14 Pct Recovery = 91% Analysis Date = 06/27/14 Pct Recovery = 91% Analysis Date = 06/22/14 Pct Recovery = 91% Analysis Date = 06/22/14 Pct Recovery = 91% Analysis Date = 06/17/14 Pct Recovery = 91% Analysis Date = 06/17/14 Pct Recovery = 91% Analysis Date = 06/13/14 Pct Recovery = 91% Analysis Date = 06/13/14 Pct Recovery = 91% Analysis Date = 06/08/14 Pct Recovery = 91% Analysis Date = 06/08/14 Pct Recovery = 91% Analysis Date = 06/03/14 Pct Recovery = 90% Analysis Date = 06/03/14 Pct Recovery = 90% Analysis Date = 05/29/14 Pct Recovery = 90% Analysis Date = 05/29/14 Pct Recovery = 90% Analysis Date = 05/24/14 Pct Recovery = 90% Analysis Date = 05/24/14 Pct Recovery = 90% Analysis Date = 05/20/14 Pct Recovery = 90% Analysis Date = 05/20/14 Pct Recovery = 90% Analysis Date = 05/15/14 Pct Recovery = 90% Analysis Date = 05/15/14 Pct Recovery = 90% Analysis Date = 05/10/14 Pct Recovery = 90% Analysis Date = 05/10/14 Pct Recovery = 90% Analysis Date = 05/05/14 Pct Recovery = 90% Analysis Date = 05/05/14 Pct Recovery = 90% Analysis Date = 05/01/14 Pct Recovery = 90% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
1,4-DICHLOROBENZENE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 48 94% 8% 94% 7%
Total 48 94% 8% 94% 7%

Sample Statistics
1,4-DICHLOROBENZENE

Characteristic N % % Basis
Plotted 48 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 48 .  
False Negatives 0 0% 0 out of 48
Not Spiked 25 .  
False Positives 0 0% 0 out of 25

BQS OBSP Determination:
1-CHLORO-1,1-DIFLUOROETHANE
METHOD: 4440 , TESTIDCODE: 85668GCM66
Open Data Set

Analysis Date = 12/12/16 SpikeMix = Accu 216041125: 40 µl & Crescent 03FF058: 40 µl Pct Recovery = 75% Analysis Date = 07/20/16 SpikeMix = Supelco LC20141V: 40 µl & Accu 216041125: 40 µl Pct Recovery = 108% Analysis Date = 07/14/16 SpikeMix = Accu 216041125: 40 µl & NSI 041816AVOC: 40 µl Pct Recovery = 88% Analysis Date = 09/08/16 SpikeMix = Supelco LC20141V: 25 µl & Accu 216041125: 25 µl Pct Recovery = 95% Analysis Date = 05/24/16 SpikeMix = Accu 216041125: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 99% Analysis Date = 03/19/15 SpikeMix = Spex Organics C1140417015: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 106% Analysis Date = 12/17/14 SpikeMix = Supelco LC06438: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 98% Analysis Date = 11/14/14 SpikeMix = Crescent 03DD004: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 96% Analysis Date = 06/10/14 SpikeMix = Crescent 03DD004: 20 µl & NSI 032614: 20 µl Pct Recovery = 86% Analysis Date = 07/13/15 SpikeMix = Crescent 04EE008: 25 µl & NSI 050515AVOC: 25 µl Pct Recovery = 83% Analysis Date = 04/09/15 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 94% Analysis Date = 08/19/14 SpikeMix = Spex Organics C1140417015: 20 µl & Accu 214031115: 20 µl Pct Recovery = 110% Analysis Date = 07/01/14 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 114% Analysis Date = 05/01/14 SpikeMix = Accu 214031115: 20 µl & NSI 032614: 20 µl Pct Recovery = 109% Analysis Date = 10/13/16 SpikeMix = Accu 216041125: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 93% Analysis Date = 08/20/16 SpikeMix = Accu 216041125: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 105% Analysis Date = 06/30/16 SpikeMix = ChemService 5082900: 15 µl & Accu 216041125: 15 µl Pct Recovery = 75% Analysis Date = 11/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 78% Analysis Date = 10/17/15 SpikeMix = Crescent 04EE008: 15 µl & NSI 050515AVOC: 15 µl Pct Recovery = 80% Analysis Date = 06/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Accu 215041380: 15 µl Pct Recovery = 95% Analysis Date = 11/06/14 SpikeMix = Spex Organics C1140417015: 10 µl & Crescent 03DD004: 10 µl Pct Recovery = 107% Analysis Date = 10/04/14 SpikeMix = Crescent 03DD004: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 102% Analysis Date = 07/29/14 SpikeMix = Crescent 03DD004: 10 µl & NSI 032614: 10 µl Pct Recovery = 107% Analysis Date = 05/03/14 SpikeMix = Crescent 03DD004: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 109% Analysis Date = 01/13/15 SpikeMix = Accu 214031115: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 106% Analysis Date = 09/09/14 SpikeMix = Accu 214031115: 10 µl & NSI 032614: 10 µl Pct Recovery = 119% Analysis Date = 07/23/14 SpikeMix = Spex Organics C1140417015: 10 µl & Accu 214031115: 10 µl Pct Recovery = 139% Analysis Date = 06/18/14 SpikeMix = Supelco LC06438: 10 µl & Accu 214031115: 10 µl Pct Recovery = 115% Analysis Date = 03/17/16 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 84% Analysis Date = 01/27/16 SpikeMix = Crescent 04EE008: 10 µl & NSI 050515AVOC: 10 µl Pct Recovery = 86% Analysis Date = 09/03/15 SpikeMix = NSI 050515AVOC: 10 µl & Spex Organics EN150428007: 10 µl Pct Recovery = 80% Analysis Date = 12/11/16 Pct Recovery = 93% Analysis Date = 12/07/16 Pct Recovery = 93% Analysis Date = 12/07/16 Pct Recovery = 93% Analysis Date = 12/02/16 Pct Recovery = 92% Analysis Date = 12/02/16 Pct Recovery = 92% Analysis Date = 11/27/16 Pct Recovery = 92% Analysis Date = 11/27/16 Pct Recovery = 92% Analysis Date = 11/22/16 Pct Recovery = 92% Analysis Date = 11/22/16 Pct Recovery = 92% Analysis Date = 11/18/16 Pct Recovery = 92% Analysis Date = 11/18/16 Pct Recovery = 92% Analysis Date = 11/13/16 Pct Recovery = 92% Analysis Date = 11/13/16 Pct Recovery = 92% Analysis Date = 11/08/16 Pct Recovery = 92% Analysis Date = 11/08/16 Pct Recovery = 92% Analysis Date = 11/03/16 Pct Recovery = 92% Analysis Date = 11/03/16 Pct Recovery = 92% Analysis Date = 10/29/16 Pct Recovery = 92% Analysis Date = 10/29/16 Pct Recovery = 92% Analysis Date = 10/25/16 Pct Recovery = 92% Analysis Date = 10/25/16 Pct Recovery = 92% Analysis Date = 10/20/16 Pct Recovery = 92% Analysis Date = 10/20/16 Pct Recovery = 92% Analysis Date = 10/15/16 Pct Recovery = 92% Analysis Date = 10/15/16 Pct Recovery = 92% Analysis Date = 10/10/16 Pct Recovery = 92% Analysis Date = 10/10/16 Pct Recovery = 92% Analysis Date = 10/06/16 Pct Recovery = 91% Analysis Date = 10/06/16 Pct Recovery = 91% Analysis Date = 10/01/16 Pct Recovery = 91% Analysis Date = 10/01/16 Pct Recovery = 91% Analysis Date = 09/26/16 Pct Recovery = 91% Analysis Date = 09/26/16 Pct Recovery = 91% Analysis Date = 09/21/16 Pct Recovery = 91% Analysis Date = 09/21/16 Pct Recovery = 91% Analysis Date = 09/16/16 Pct Recovery = 91% Analysis Date = 09/16/16 Pct Recovery = 91% Analysis Date = 09/12/16 Pct Recovery = 91% Analysis Date = 09/12/16 Pct Recovery = 91% Analysis Date = 09/07/16 Pct Recovery = 91% Analysis Date = 09/07/16 Pct Recovery = 91% Analysis Date = 09/02/16 Pct Recovery = 91% Analysis Date = 09/02/16 Pct Recovery = 91% Analysis Date = 08/28/16 Pct Recovery = 91% Analysis Date = 08/28/16 Pct Recovery = 91% Analysis Date = 08/24/16 Pct Recovery = 91% Analysis Date = 08/24/16 Pct Recovery = 91% Analysis Date = 08/19/16 Pct Recovery = 91% Analysis Date = 08/19/16 Pct Recovery = 91% Analysis Date = 08/14/16 Pct Recovery = 91% Analysis Date = 08/14/16 Pct Recovery = 91% Analysis Date = 08/09/16 Pct Recovery = 91% Analysis Date = 08/09/16 Pct Recovery = 91% Analysis Date = 08/04/16 Pct Recovery = 90% Analysis Date = 08/04/16 Pct Recovery = 90% Analysis Date = 07/31/16 Pct Recovery = 90% Analysis Date = 07/31/16 Pct Recovery = 90% Analysis Date = 07/26/16 Pct Recovery = 90% Analysis Date = 07/26/16 Pct Recovery = 90% Analysis Date = 07/21/16 Pct Recovery = 90% Analysis Date = 07/21/16 Pct Recovery = 90% Analysis Date = 07/16/16 Pct Recovery = 90% Analysis Date = 07/16/16 Pct Recovery = 90% Analysis Date = 07/12/16 Pct Recovery = 90% Analysis Date = 07/12/16 Pct Recovery = 90% Analysis Date = 07/07/16 Pct Recovery = 90% Analysis Date = 07/07/16 Pct Recovery = 90% Analysis Date = 07/02/16 Pct Recovery = 90% Analysis Date = 07/02/16 Pct Recovery = 90% Analysis Date = 06/27/16 Pct Recovery = 90% Analysis Date = 06/27/16 Pct Recovery = 90% Analysis Date = 06/22/16 Pct Recovery = 90% Analysis Date = 06/22/16 Pct Recovery = 90% Analysis Date = 06/18/16 Pct Recovery = 90% Analysis Date = 06/18/16 Pct Recovery = 90% Analysis Date = 06/13/16 Pct Recovery = 90% Analysis Date = 06/13/16 Pct Recovery = 90% Analysis Date = 06/08/16 Pct Recovery = 90% Analysis Date = 06/08/16 Pct Recovery = 90% Analysis Date = 06/03/16 Pct Recovery = 89% Analysis Date = 06/03/16 Pct Recovery = 89% Analysis Date = 05/30/16 Pct Recovery = 89% Analysis Date = 05/30/16 Pct Recovery = 89% Analysis Date = 05/25/16 Pct Recovery = 89% Analysis Date = 05/25/16 Pct Recovery = 89% Analysis Date = 05/20/16 Pct Recovery = 89% Analysis Date = 05/20/16 Pct Recovery = 89% Analysis Date = 05/15/16 Pct Recovery = 89% Analysis Date = 05/15/16 Pct Recovery = 89% Analysis Date = 05/10/16 Pct Recovery = 89% Analysis Date = 05/10/16 Pct Recovery = 89% Analysis Date = 05/06/16 Pct Recovery = 89% Analysis Date = 05/06/16 Pct Recovery = 89% Analysis Date = 05/01/16 Pct Recovery = 89% Analysis Date = 05/01/16 Pct Recovery = 89% Analysis Date = 04/26/16 Pct Recovery = 89% Analysis Date = 04/26/16 Pct Recovery = 89% Analysis Date = 04/21/16 Pct Recovery = 89% Analysis Date = 04/21/16 Pct Recovery = 89% Analysis Date = 04/16/16 Pct Recovery = 89% Analysis Date = 04/16/16 Pct Recovery = 89% Analysis Date = 04/12/16 Pct Recovery = 89% Analysis Date = 04/12/16 Pct Recovery = 89% Analysis Date = 04/07/16 Pct Recovery = 89% Analysis Date = 04/07/16 Pct Recovery = 89% Analysis Date = 04/02/16 Pct Recovery = 88% Analysis Date = 04/02/16 Pct Recovery = 88% Analysis Date = 03/28/16 Pct Recovery = 88% Analysis Date = 03/28/16 Pct Recovery = 88% Analysis Date = 03/24/16 Pct Recovery = 88% Analysis Date = 03/24/16 Pct Recovery = 88% Analysis Date = 03/19/16 Pct Recovery = 88% Analysis Date = 03/19/16 Pct Recovery = 88% Analysis Date = 03/14/16 Pct Recovery = 88% Analysis Date = 03/14/16 Pct Recovery = 88% Analysis Date = 03/09/16 Pct Recovery = 88% Analysis Date = 03/09/16 Pct Recovery = 88% Analysis Date = 03/04/16 Pct Recovery = 88% Analysis Date = 03/04/16 Pct Recovery = 88% Analysis Date = 02/29/16 Pct Recovery = 88% Analysis Date = 02/29/16 Pct Recovery = 88% Analysis Date = 02/24/16 Pct Recovery = 88% Analysis Date = 02/24/16 Pct Recovery = 88% Analysis Date = 02/19/16 Pct Recovery = 88% Analysis Date = 02/19/16 Pct Recovery = 88% Analysis Date = 02/14/16 Pct Recovery = 88% Analysis Date = 02/14/16 Pct Recovery = 88% Analysis Date = 02/10/16 Pct Recovery = 88% Analysis Date = 02/10/16 Pct Recovery = 88% Analysis Date = 02/05/16 Pct Recovery = 88% Analysis Date = 02/05/16 Pct Recovery = 88% Analysis Date = 01/31/16 Pct Recovery = 87% Analysis Date = 01/31/16 Pct Recovery = 87% Analysis Date = 01/26/16 Pct Recovery = 87% Analysis Date = 01/26/16 Pct Recovery = 87% Analysis Date = 01/21/16 Pct Recovery = 87% Analysis Date = 01/21/16 Pct Recovery = 87% Analysis Date = 01/17/16 Pct Recovery = 87% Analysis Date = 01/17/16 Pct Recovery = 87% Analysis Date = 01/12/16 Pct Recovery = 87% Analysis Date = 01/12/16 Pct Recovery = 87% Analysis Date = 01/07/16 Pct Recovery = 87% Analysis Date = 01/07/16 Pct Recovery = 87% Analysis Date = 01/02/16 Pct Recovery = 87% Analysis Date = 01/02/16 Pct Recovery = 87% Analysis Date = 12/29/15 Pct Recovery = 87% Analysis Date = 12/29/15 Pct Recovery = 87% Analysis Date = 12/24/15 Pct Recovery = 87% Analysis Date = 12/24/15 Pct Recovery = 87% Analysis Date = 12/19/15 Pct Recovery = 87% Analysis Date = 12/19/15 Pct Recovery = 87% Analysis Date = 12/14/15 Pct Recovery = 87% Analysis Date = 12/14/15 Pct Recovery = 87% Analysis Date = 12/09/15 Pct Recovery = 87% Analysis Date = 12/09/15 Pct Recovery = 87% Analysis Date = 12/05/15 Pct Recovery = 87% Analysis Date = 12/05/15 Pct Recovery = 87% Analysis Date = 11/30/15 Pct Recovery = 87% Analysis Date = 11/30/15 Pct Recovery = 87% Analysis Date = 11/25/15 Pct Recovery = 87% Analysis Date = 11/25/15 Pct Recovery = 87% Analysis Date = 11/20/15 Pct Recovery = 87% Analysis Date = 11/20/15 Pct Recovery = 87% Analysis Date = 11/16/15 Pct Recovery = 87% Analysis Date = 11/16/15 Pct Recovery = 87% Analysis Date = 11/11/15 Pct Recovery = 87% Analysis Date = 11/11/15 Pct Recovery = 87% Analysis Date = 11/06/15 Pct Recovery = 87% Analysis Date = 11/06/15 Pct Recovery = 87% Analysis Date = 11/01/15 Pct Recovery = 86% Analysis Date = 11/01/15 Pct Recovery = 86% Analysis Date = 10/27/15 Pct Recovery = 86% Analysis Date = 10/27/15 Pct Recovery = 86% Analysis Date = 10/23/15 Pct Recovery = 86% Analysis Date = 10/23/15 Pct Recovery = 86% Analysis Date = 10/18/15 Pct Recovery = 86% Analysis Date = 10/18/15 Pct Recovery = 86% Analysis Date = 10/13/15 Pct Recovery = 86% Analysis Date = 10/13/15 Pct Recovery = 86% Analysis Date = 10/08/15 Pct Recovery = 87% Analysis Date = 10/08/15 Pct Recovery = 87% Analysis Date = 10/04/15 Pct Recovery = 87% Analysis Date = 10/04/15 Pct Recovery = 87% Analysis Date = 09/29/15 Pct Recovery = 87% Analysis Date = 09/29/15 Pct Recovery = 87% Analysis Date = 09/24/15 Pct Recovery = 87% Analysis Date = 09/24/15 Pct Recovery = 87% Analysis Date = 09/19/15 Pct Recovery = 87% Analysis Date = 09/19/15 Pct Recovery = 87% Analysis Date = 09/14/15 Pct Recovery = 87% Analysis Date = 09/14/15 Pct Recovery = 87% Analysis Date = 09/10/15 Pct Recovery = 87% Analysis Date = 09/10/15 Pct Recovery = 87% Analysis Date = 09/05/15 Pct Recovery = 88% Analysis Date = 09/05/15 Pct Recovery = 88% Analysis Date = 08/31/15 Pct Recovery = 88% Analysis Date = 08/31/15 Pct Recovery = 88% Analysis Date = 08/26/15 Pct Recovery = 88% Analysis Date = 08/26/15 Pct Recovery = 88% Analysis Date = 08/21/15 Pct Recovery = 88% Analysis Date = 08/21/15 Pct Recovery = 88% Analysis Date = 08/17/15 Pct Recovery = 88% Analysis Date = 08/17/15 Pct Recovery = 88% Analysis Date = 08/12/15 Pct Recovery = 88% Analysis Date = 08/12/15 Pct Recovery = 88% Analysis Date = 08/07/15 Pct Recovery = 88% Analysis Date = 08/07/15 Pct Recovery = 88% Analysis Date = 08/02/15 Pct Recovery = 89% Analysis Date = 08/02/15 Pct Recovery = 89% Analysis Date = 07/29/15 Pct Recovery = 89% Analysis Date = 07/29/15 Pct Recovery = 89% Analysis Date = 07/24/15 Pct Recovery = 89% Analysis Date = 07/24/15 Pct Recovery = 89% Analysis Date = 07/19/15 Pct Recovery = 89% Analysis Date = 07/19/15 Pct Recovery = 89% Analysis Date = 07/14/15 Pct Recovery = 89% Analysis Date = 07/14/15 Pct Recovery = 89% Analysis Date = 07/09/15 Pct Recovery = 89% Analysis Date = 07/09/15 Pct Recovery = 89% Analysis Date = 07/05/15 Pct Recovery = 90% Analysis Date = 07/05/15 Pct Recovery = 90% Analysis Date = 06/30/15 Pct Recovery = 90% Analysis Date = 06/30/15 Pct Recovery = 90% Analysis Date = 06/25/15 Pct Recovery = 90% Analysis Date = 06/25/15 Pct Recovery = 90% Analysis Date = 06/20/15 Pct Recovery = 91% Analysis Date = 06/20/15 Pct Recovery = 91% Analysis Date = 06/16/15 Pct Recovery = 91% Analysis Date = 06/16/15 Pct Recovery = 91% Analysis Date = 06/11/15 Pct Recovery = 91% Analysis Date = 06/11/15 Pct Recovery = 91% Analysis Date = 06/06/15 Pct Recovery = 91% Analysis Date = 06/06/15 Pct Recovery = 91% Analysis Date = 06/01/15 Pct Recovery = 92% Analysis Date = 06/01/15 Pct Recovery = 92% Analysis Date = 05/27/15 Pct Recovery = 92% Analysis Date = 05/27/15 Pct Recovery = 92% Analysis Date = 05/23/15 Pct Recovery = 92% Analysis Date = 05/23/15 Pct Recovery = 92% Analysis Date = 05/18/15 Pct Recovery = 92% Analysis Date = 05/18/15 Pct Recovery = 92% Analysis Date = 05/13/15 Pct Recovery = 93% Analysis Date = 05/13/15 Pct Recovery = 93% Analysis Date = 05/08/15 Pct Recovery = 93% Analysis Date = 05/08/15 Pct Recovery = 93% Analysis Date = 05/04/15 Pct Recovery = 93% Analysis Date = 05/04/15 Pct Recovery = 93% Analysis Date = 04/29/15 Pct Recovery = 94% Analysis Date = 04/29/15 Pct Recovery = 94% Analysis Date = 04/24/15 Pct Recovery = 94% Analysis Date = 04/24/15 Pct Recovery = 94% Analysis Date = 04/19/15 Pct Recovery = 94% Analysis Date = 04/19/15 Pct Recovery = 94% Analysis Date = 04/14/15 Pct Recovery = 94% Analysis Date = 04/14/15 Pct Recovery = 94% Analysis Date = 04/10/15 Pct Recovery = 95% Analysis Date = 04/10/15 Pct Recovery = 95% Analysis Date = 04/05/15 Pct Recovery = 95% Analysis Date = 04/05/15 Pct Recovery = 95% Analysis Date = 03/31/15 Pct Recovery = 95% Analysis Date = 03/31/15 Pct Recovery = 95% Analysis Date = 03/26/15 Pct Recovery = 96% Analysis Date = 03/26/15 Pct Recovery = 96% Analysis Date = 03/22/15 Pct Recovery = 96% Analysis Date = 03/22/15 Pct Recovery = 96% Analysis Date = 03/17/15 Pct Recovery = 97% Analysis Date = 03/17/15 Pct Recovery = 97% Analysis Date = 03/12/15 Pct Recovery = 97% Analysis Date = 03/12/15 Pct Recovery = 97% Analysis Date = 03/07/15 Pct Recovery = 97% Analysis Date = 03/07/15 Pct Recovery = 97% Analysis Date = 03/02/15 Pct Recovery = 98% Analysis Date = 03/02/15 Pct Recovery = 98% Analysis Date = 02/26/15 Pct Recovery = 98% Analysis Date = 02/26/15 Pct Recovery = 98% Analysis Date = 02/21/15 Pct Recovery = 99% Analysis Date = 02/21/15 Pct Recovery = 99% Analysis Date = 02/16/15 Pct Recovery = 99% Analysis Date = 02/16/15 Pct Recovery = 99% Analysis Date = 02/11/15 Pct Recovery = 99% Analysis Date = 02/11/15 Pct Recovery = 99% Analysis Date = 02/07/15 Pct Recovery = 100% Analysis Date = 02/07/15 Pct Recovery = 100% Analysis Date = 02/02/15 Pct Recovery = 100% Analysis Date = 02/02/15 Pct Recovery = 100% Analysis Date = 01/28/15 Pct Recovery = 101% Analysis Date = 01/28/15 Pct Recovery = 101% Analysis Date = 01/23/15 Pct Recovery = 101% Analysis Date = 01/23/15 Pct Recovery = 101% Analysis Date = 01/18/15 Pct Recovery = 101% Analysis Date = 01/18/15 Pct Recovery = 101% Analysis Date = 01/14/15 Pct Recovery = 102% Analysis Date = 01/14/15 Pct Recovery = 102% Analysis Date = 01/09/15 Pct Recovery = 102% Analysis Date = 01/09/15 Pct Recovery = 102% Analysis Date = 01/04/15 Pct Recovery = 102% Analysis Date = 01/04/15 Pct Recovery = 102% Analysis Date = 12/30/14 Pct Recovery = 103% Analysis Date = 12/30/14 Pct Recovery = 103% Analysis Date = 12/25/14 Pct Recovery = 103% Analysis Date = 12/25/14 Pct Recovery = 103% Analysis Date = 12/21/14 Pct Recovery = 103% Analysis Date = 12/21/14 Pct Recovery = 103% Analysis Date = 12/16/14 Pct Recovery = 104% Analysis Date = 12/16/14 Pct Recovery = 104% Analysis Date = 12/11/14 Pct Recovery = 104% Analysis Date = 12/11/14 Pct Recovery = 104% Analysis Date = 12/06/14 Pct Recovery = 104% Analysis Date = 12/06/14 Pct Recovery = 104% Analysis Date = 12/02/14 Pct Recovery = 105% Analysis Date = 12/02/14 Pct Recovery = 105% Analysis Date = 11/27/14 Pct Recovery = 105% Analysis Date = 11/27/14 Pct Recovery = 105% Analysis Date = 11/22/14 Pct Recovery = 105% Analysis Date = 11/22/14 Pct Recovery = 105% Analysis Date = 11/17/14 Pct Recovery = 105% Analysis Date = 11/17/14 Pct Recovery = 105% Analysis Date = 11/12/14 Pct Recovery = 106% Analysis Date = 11/12/14 Pct Recovery = 106% Analysis Date = 11/08/14 Pct Recovery = 106% Analysis Date = 11/08/14 Pct Recovery = 106% Analysis Date = 11/03/14 Pct Recovery = 106% Analysis Date = 11/03/14 Pct Recovery = 106% Analysis Date = 10/29/14 Pct Recovery = 106% Analysis Date = 10/29/14 Pct Recovery = 106% Analysis Date = 10/24/14 Pct Recovery = 106% Analysis Date = 10/24/14 Pct Recovery = 106% Analysis Date = 10/20/14 Pct Recovery = 107% Analysis Date = 10/20/14 Pct Recovery = 107% Analysis Date = 10/15/14 Pct Recovery = 107% Analysis Date = 10/15/14 Pct Recovery = 107% Analysis Date = 10/10/14 Pct Recovery = 107% Analysis Date = 10/10/14 Pct Recovery = 107% Analysis Date = 10/05/14 Pct Recovery = 107% Analysis Date = 10/05/14 Pct Recovery = 107% Analysis Date = 09/30/14 Pct Recovery = 107% Analysis Date = 09/30/14 Pct Recovery = 107% Analysis Date = 09/26/14 Pct Recovery = 107% Analysis Date = 09/26/14 Pct Recovery = 107% Analysis Date = 09/21/14 Pct Recovery = 108% Analysis Date = 09/21/14 Pct Recovery = 108% Analysis Date = 09/16/14 Pct Recovery = 108% Analysis Date = 09/16/14 Pct Recovery = 108% Analysis Date = 09/11/14 Pct Recovery = 108% Analysis Date = 09/11/14 Pct Recovery = 108% Analysis Date = 09/07/14 Pct Recovery = 108% Analysis Date = 09/07/14 Pct Recovery = 108% Analysis Date = 09/02/14 Pct Recovery = 108% Analysis Date = 09/02/14 Pct Recovery = 108% Analysis Date = 08/28/14 Pct Recovery = 108% Analysis Date = 08/28/14 Pct Recovery = 108% Analysis Date = 08/23/14 Pct Recovery = 108% Analysis Date = 08/23/14 Pct Recovery = 108% Analysis Date = 08/18/14 Pct Recovery = 109% Analysis Date = 08/18/14 Pct Recovery = 109% Analysis Date = 08/14/14 Pct Recovery = 109% Analysis Date = 08/14/14 Pct Recovery = 109% Analysis Date = 08/09/14 Pct Recovery = 109% Analysis Date = 08/09/14 Pct Recovery = 109% Analysis Date = 08/04/14 Pct Recovery = 109% Analysis Date = 08/04/14 Pct Recovery = 109% Analysis Date = 07/30/14 Pct Recovery = 109% Analysis Date = 07/30/14 Pct Recovery = 109% Analysis Date = 07/26/14 Pct Recovery = 109% Analysis Date = 07/26/14 Pct Recovery = 109% Analysis Date = 07/21/14 Pct Recovery = 110% Analysis Date = 07/21/14 Pct Recovery = 110% Analysis Date = 07/16/14 Pct Recovery = 110% Analysis Date = 07/16/14 Pct Recovery = 110% Analysis Date = 07/11/14 Pct Recovery = 110% Analysis Date = 07/11/14 Pct Recovery = 110% Analysis Date = 07/06/14 Pct Recovery = 110% Analysis Date = 07/06/14 Pct Recovery = 110% Analysis Date = 07/02/14 Pct Recovery = 110% Analysis Date = 07/02/14 Pct Recovery = 110% Analysis Date = 06/27/14 Pct Recovery = 110% Analysis Date = 06/27/14 Pct Recovery = 110% Analysis Date = 06/22/14 Pct Recovery = 110% Analysis Date = 06/22/14 Pct Recovery = 110% Analysis Date = 06/17/14 Pct Recovery = 111% Analysis Date = 06/17/14 Pct Recovery = 111% Analysis Date = 06/13/14 Pct Recovery = 111% Analysis Date = 06/13/14 Pct Recovery = 111% Analysis Date = 06/08/14 Pct Recovery = 111% Analysis Date = 06/08/14 Pct Recovery = 111% Analysis Date = 06/03/14 Pct Recovery = 111% Analysis Date = 06/03/14 Pct Recovery = 111% Analysis Date = 05/29/14 Pct Recovery = 111% Analysis Date = 05/29/14 Pct Recovery = 111% Analysis Date = 05/24/14 Pct Recovery = 111% Analysis Date = 05/24/14 Pct Recovery = 111% Analysis Date = 05/20/14 Pct Recovery = 111% Analysis Date = 05/20/14 Pct Recovery = 111% Analysis Date = 05/15/14 Pct Recovery = 111% Analysis Date = 05/15/14 Pct Recovery = 111% Analysis Date = 05/10/14 Pct Recovery = 112% Analysis Date = 05/10/14 Pct Recovery = 112% Analysis Date = 05/05/14 Pct Recovery = 112% Analysis Date = 05/05/14 Pct Recovery = 112% Analysis Date = 05/01/14 Pct Recovery = 112% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
1-CHLORO-1,1-DIFLUOROETHANE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 31 98% 15% 98% 17%
Total 31 98% 15% 98% 17%

Sample Statistics
1-CHLORO-1,1-DIFLUOROETHANE

Characteristic N % % Basis
Plotted 31 97% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 32 .  
False Negatives 1 3% 1 out of 32
Not Spiked 41 .  
False Positives 0 0% 0 out of 41

BQS OBSP Determination:
2,2-DICHLORO-1,1,1-TRIFLUOROETHANE
METHOD: 4440 , TESTIDCODE: 62174GCM66
Open Data Set

Analysis Date = 12/12/16 SpikeMix = Accu 216041125: 40 µl & Crescent 03FF058: 40 µl Pct Recovery = 101% Analysis Date = 07/20/16 SpikeMix = Supelco LC20141V: 40 µl & Accu 216041125: 40 µl Pct Recovery = 109% Analysis Date = 07/14/16 SpikeMix = Accu 216041125: 40 µl & NSI 041816AVOC: 40 µl Pct Recovery = 96% Analysis Date = 09/08/16 SpikeMix = Supelco LC20141V: 25 µl & Accu 216041125: 25 µl Pct Recovery = 89% Analysis Date = 05/24/16 SpikeMix = Accu 216041125: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 102% Analysis Date = 03/19/15 SpikeMix = Spex Organics C1140417015: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 116% Analysis Date = 12/17/14 SpikeMix = Supelco LC06438: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 96% Analysis Date = 11/14/14 SpikeMix = Crescent 03DD004: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 95% Analysis Date = 06/10/14 SpikeMix = Crescent 03DD004: 20 µl & NSI 032614: 20 µl Pct Recovery = 108% Analysis Date = 08/15/15 SpikeMix = Supelco LC13545: 25 µl & Crescent 04EE008: 25 µl Pct Recovery = 111% Analysis Date = 06/16/15 SpikeMix = ERA 0406-15-03: 25 µl & Supelco LC13545: 25 µl Pct Recovery = 103% Analysis Date = 04/09/15 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 112% Analysis Date = 08/19/14 SpikeMix = Spex Organics C1140417015: 20 µl & Accu 214031115: 20 µl Pct Recovery = 107% Analysis Date = 07/01/14 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 110% Analysis Date = 05/01/14 SpikeMix = Accu 214031115: 20 µl & NSI 032614: 20 µl Pct Recovery = 111% Analysis Date = 10/13/16 SpikeMix = Accu 216041125: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 106% Analysis Date = 08/20/16 SpikeMix = Accu 216041125: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 105% Analysis Date = 06/30/16 SpikeMix = ChemService 5082900: 15 µl & Accu 216041125: 15 µl Pct Recovery = 76% Analysis Date = 04/26/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 102% Analysis Date = 02/05/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 112% Analysis Date = 11/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 103% Analysis Date = 10/16/15 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 114% Analysis Date = 05/09/15 SpikeMix = Spex Organics EN150428007: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 123% Analysis Date = 04/02/16 SpikeMix = Supelco LC13545: 15 µl & Accu 215041380: 15 µl Pct Recovery = 96% Analysis Date = 12/18/15 SpikeMix = Supelco LC13545: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 85% Analysis Date = 11/06/14 SpikeMix = Spex Organics C1140417015: 10 µl & Crescent 03DD004: 10 µl Pct Recovery = 104% Analysis Date = 10/04/14 SpikeMix = Crescent 03DD004: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 111% Analysis Date = 07/29/14 SpikeMix = Crescent 03DD004: 10 µl & NSI 032614: 10 µl Pct Recovery = 114% Analysis Date = 05/03/14 SpikeMix = Crescent 03DD004: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 113% Analysis Date = 02/18/16 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 108% Analysis Date = 11/12/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 124% Analysis Date = 09/03/15 SpikeMix = NSI 050515AVOC: 10 µl & Spex Organics EN150428007: 10 µl Pct Recovery = 113% Analysis Date = 05/21/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 132% Analysis Date = 05/13/16 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 108% Analysis Date = 03/17/16 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 88% Analysis Date = 12/10/15 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 111% Analysis Date = 06/27/15 SpikeMix = ERA 0406-15-03: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 99% Analysis Date = 05/09/15 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 100% Analysis Date = 01/13/15 SpikeMix = Accu 214031115: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 93% Analysis Date = 09/09/14 SpikeMix = Accu 214031115: 10 µl & NSI 032614: 10 µl Pct Recovery = 106% Analysis Date = 07/23/14 SpikeMix = Spex Organics C1140417015: 10 µl & Accu 214031115: 10 µl Pct Recovery = 139% Analysis Date = 06/18/14 SpikeMix = Supelco LC06438: 10 µl & Accu 214031115: 10 µl Pct Recovery = 113% Analysis Date = 12/11/16 Pct Recovery = 96% Analysis Date = 12/07/16 Pct Recovery = 97% Analysis Date = 12/07/16 Pct Recovery = 97% Analysis Date = 12/02/16 Pct Recovery = 97% Analysis Date = 12/02/16 Pct Recovery = 97% Analysis Date = 11/27/16 Pct Recovery = 97% Analysis Date = 11/27/16 Pct Recovery = 97% Analysis Date = 11/22/16 Pct Recovery = 97% Analysis Date = 11/22/16 Pct Recovery = 97% Analysis Date = 11/18/16 Pct Recovery = 97% Analysis Date = 11/18/16 Pct Recovery = 97% Analysis Date = 11/13/16 Pct Recovery = 97% Analysis Date = 11/13/16 Pct Recovery = 97% Analysis Date = 11/08/16 Pct Recovery = 97% Analysis Date = 11/08/16 Pct Recovery = 97% Analysis Date = 11/03/16 Pct Recovery = 97% Analysis Date = 11/03/16 Pct Recovery = 97% Analysis Date = 10/29/16 Pct Recovery = 97% Analysis Date = 10/29/16 Pct Recovery = 97% Analysis Date = 10/25/16 Pct Recovery = 97% Analysis Date = 10/25/16 Pct Recovery = 97% Analysis Date = 10/20/16 Pct Recovery = 97% Analysis Date = 10/20/16 Pct Recovery = 97% Analysis Date = 10/15/16 Pct Recovery = 98% Analysis Date = 10/15/16 Pct Recovery = 98% Analysis Date = 10/10/16 Pct Recovery = 98% Analysis Date = 10/10/16 Pct Recovery = 98% Analysis Date = 10/06/16 Pct Recovery = 98% Analysis Date = 10/06/16 Pct Recovery = 98% Analysis Date = 10/01/16 Pct Recovery = 98% Analysis Date = 10/01/16 Pct Recovery = 98% Analysis Date = 09/26/16 Pct Recovery = 98% Analysis Date = 09/26/16 Pct Recovery = 98% Analysis Date = 09/21/16 Pct Recovery = 98% Analysis Date = 09/21/16 Pct Recovery = 98% Analysis Date = 09/16/16 Pct Recovery = 98% Analysis Date = 09/16/16 Pct Recovery = 98% Analysis Date = 09/12/16 Pct Recovery = 98% Analysis Date = 09/12/16 Pct Recovery = 98% Analysis Date = 09/07/16 Pct Recovery = 98% Analysis Date = 09/07/16 Pct Recovery = 98% Analysis Date = 09/02/16 Pct Recovery = 98% Analysis Date = 09/02/16 Pct Recovery = 98% Analysis Date = 08/28/16 Pct Recovery = 98% Analysis Date = 08/28/16 Pct Recovery = 98% Analysis Date = 08/24/16 Pct Recovery = 98% Analysis Date = 08/24/16 Pct Recovery = 98% Analysis Date = 08/19/16 Pct Recovery = 99% Analysis Date = 08/19/16 Pct Recovery = 99% Analysis Date = 08/14/16 Pct Recovery = 99% Analysis Date = 08/14/16 Pct Recovery = 99% Analysis Date = 08/09/16 Pct Recovery = 99% Analysis Date = 08/09/16 Pct Recovery = 99% Analysis Date = 08/04/16 Pct Recovery = 99% Analysis Date = 08/04/16 Pct Recovery = 99% Analysis Date = 07/31/16 Pct Recovery = 99% Analysis Date = 07/31/16 Pct Recovery = 99% Analysis Date = 07/26/16 Pct Recovery = 99% Analysis Date = 07/26/16 Pct Recovery = 99% Analysis Date = 07/21/16 Pct Recovery = 99% Analysis Date = 07/21/16 Pct Recovery = 99% Analysis Date = 07/16/16 Pct Recovery = 99% Analysis Date = 07/16/16 Pct Recovery = 99% Analysis Date = 07/12/16 Pct Recovery = 99% Analysis Date = 07/12/16 Pct Recovery = 99% Analysis Date = 07/07/16 Pct Recovery = 99% Analysis Date = 07/07/16 Pct Recovery = 99% Analysis Date = 07/02/16 Pct Recovery = 99% Analysis Date = 07/02/16 Pct Recovery = 99% Analysis Date = 06/27/16 Pct Recovery = 100% Analysis Date = 06/27/16 Pct Recovery = 100% Analysis Date = 06/22/16 Pct Recovery = 100% Analysis Date = 06/22/16 Pct Recovery = 100% Analysis Date = 06/18/16 Pct Recovery = 100% Analysis Date = 06/18/16 Pct Recovery = 100% Analysis Date = 06/13/16 Pct Recovery = 100% Analysis Date = 06/13/16 Pct Recovery = 100% Analysis Date = 06/08/16 Pct Recovery = 100% Analysis Date = 06/08/16 Pct Recovery = 100% Analysis Date = 06/03/16 Pct Recovery = 100% Analysis Date = 06/03/16 Pct Recovery = 100% Analysis Date = 05/30/16 Pct Recovery = 100% Analysis Date = 05/30/16 Pct Recovery = 100% Analysis Date = 05/25/16 Pct Recovery = 100% Analysis Date = 05/25/16 Pct Recovery = 100% Analysis Date = 05/20/16 Pct Recovery = 100% Analysis Date = 05/20/16 Pct Recovery = 100% Analysis Date = 05/15/16 Pct Recovery = 101% Analysis Date = 05/15/16 Pct Recovery = 101% Analysis Date = 05/10/16 Pct Recovery = 101% Analysis Date = 05/10/16 Pct Recovery = 101% Analysis Date = 05/06/16 Pct Recovery = 101% Analysis Date = 05/06/16 Pct Recovery = 101% Analysis Date = 05/01/16 Pct Recovery = 101% Analysis Date = 05/01/16 Pct Recovery = 101% Analysis Date = 04/26/16 Pct Recovery = 101% Analysis Date = 04/26/16 Pct Recovery = 101% Analysis Date = 04/21/16 Pct Recovery = 101% Analysis Date = 04/21/16 Pct Recovery = 101% Analysis Date = 04/16/16 Pct Recovery = 101% Analysis Date = 04/16/16 Pct Recovery = 101% Analysis Date = 04/12/16 Pct Recovery = 101% Analysis Date = 04/12/16 Pct Recovery = 101% Analysis Date = 04/07/16 Pct Recovery = 101% Analysis Date = 04/07/16 Pct Recovery = 101% Analysis Date = 04/02/16 Pct Recovery = 102% Analysis Date = 04/02/16 Pct Recovery = 102% Analysis Date = 03/28/16 Pct Recovery = 102% Analysis Date = 03/28/16 Pct Recovery = 102% Analysis Date = 03/24/16 Pct Recovery = 102% Analysis Date = 03/24/16 Pct Recovery = 102% Analysis Date = 03/19/16 Pct Recovery = 102% Analysis Date = 03/19/16 Pct Recovery = 102% Analysis Date = 03/14/16 Pct Recovery = 102% Analysis Date = 03/14/16 Pct Recovery = 102% Analysis Date = 03/09/16 Pct Recovery = 102% Analysis Date = 03/09/16 Pct Recovery = 102% Analysis Date = 03/04/16 Pct Recovery = 103% Analysis Date = 03/04/16 Pct Recovery = 103% Analysis Date = 02/29/16 Pct Recovery = 103% Analysis Date = 02/29/16 Pct Recovery = 103% Analysis Date = 02/24/16 Pct Recovery = 103% Analysis Date = 02/24/16 Pct Recovery = 103% Analysis Date = 02/19/16 Pct Recovery = 103% Analysis Date = 02/19/16 Pct Recovery = 103% Analysis Date = 02/14/16 Pct Recovery = 103% Analysis Date = 02/14/16 Pct Recovery = 103% Analysis Date = 02/10/16 Pct Recovery = 103% Analysis Date = 02/10/16 Pct Recovery = 103% Analysis Date = 02/05/16 Pct Recovery = 104% Analysis Date = 02/05/16 Pct Recovery = 104% Analysis Date = 01/31/16 Pct Recovery = 104% Analysis Date = 01/31/16 Pct Recovery = 104% Analysis Date = 01/26/16 Pct Recovery = 104% Analysis Date = 01/26/16 Pct Recovery = 104% Analysis Date = 01/21/16 Pct Recovery = 104% Analysis Date = 01/21/16 Pct Recovery = 104% Analysis Date = 01/17/16 Pct Recovery = 104% Analysis Date = 01/17/16 Pct Recovery = 104% Analysis Date = 01/12/16 Pct Recovery = 105% Analysis Date = 01/12/16 Pct Recovery = 105% Analysis Date = 01/07/16 Pct Recovery = 105% Analysis Date = 01/07/16 Pct Recovery = 105% Analysis Date = 01/02/16 Pct Recovery = 105% Analysis Date = 01/02/16 Pct Recovery = 105% Analysis Date = 12/29/15 Pct Recovery = 105% Analysis Date = 12/29/15 Pct Recovery = 105% Analysis Date = 12/24/15 Pct Recovery = 105% Analysis Date = 12/24/15 Pct Recovery = 105% Analysis Date = 12/19/15 Pct Recovery = 105% Analysis Date = 12/19/15 Pct Recovery = 105% Analysis Date = 12/14/15 Pct Recovery = 106% Analysis Date = 12/14/15 Pct Recovery = 106% Analysis Date = 12/09/15 Pct Recovery = 106% Analysis Date = 12/09/15 Pct Recovery = 106% Analysis Date = 12/05/15 Pct Recovery = 106% Analysis Date = 12/05/15 Pct Recovery = 106% Analysis Date = 11/30/15 Pct Recovery = 106% Analysis Date = 11/30/15 Pct Recovery = 106% Analysis Date = 11/25/15 Pct Recovery = 106% Analysis Date = 11/25/15 Pct Recovery = 106% Analysis Date = 11/20/15 Pct Recovery = 106% Analysis Date = 11/20/15 Pct Recovery = 106% Analysis Date = 11/16/15 Pct Recovery = 107% Analysis Date = 11/16/15 Pct Recovery = 107% Analysis Date = 11/11/15 Pct Recovery = 107% Analysis Date = 11/11/15 Pct Recovery = 107% Analysis Date = 11/06/15 Pct Recovery = 107% Analysis Date = 11/06/15 Pct Recovery = 107% Analysis Date = 11/01/15 Pct Recovery = 107% Analysis Date = 11/01/15 Pct Recovery = 107% Analysis Date = 10/27/15 Pct Recovery = 107% Analysis Date = 10/27/15 Pct Recovery = 107% Analysis Date = 10/23/15 Pct Recovery = 108% Analysis Date = 10/23/15 Pct Recovery = 108% Analysis Date = 10/18/15 Pct Recovery = 108% Analysis Date = 10/18/15 Pct Recovery = 108% Analysis Date = 10/13/15 Pct Recovery = 108% Analysis Date = 10/13/15 Pct Recovery = 108% Analysis Date = 10/08/15 Pct Recovery = 108% Analysis Date = 10/08/15 Pct Recovery = 108% Analysis Date = 10/04/15 Pct Recovery = 108% Analysis Date = 10/04/15 Pct Recovery = 108% Analysis Date = 09/29/15 Pct Recovery = 108% Analysis Date = 09/29/15 Pct Recovery = 108% Analysis Date = 09/24/15 Pct Recovery = 108% Analysis Date = 09/24/15 Pct Recovery = 108% Analysis Date = 09/19/15 Pct Recovery = 108% Analysis Date = 09/19/15 Pct Recovery = 108% Analysis Date = 09/14/15 Pct Recovery = 108% Analysis Date = 09/14/15 Pct Recovery = 108% Analysis Date = 09/10/15 Pct Recovery = 108% Analysis Date = 09/10/15 Pct Recovery = 108% Analysis Date = 09/05/15 Pct Recovery = 108% Analysis Date = 09/05/15 Pct Recovery = 108% Analysis Date = 08/31/15 Pct Recovery = 108% Analysis Date = 08/31/15 Pct Recovery = 108% Analysis Date = 08/26/15 Pct Recovery = 109% Analysis Date = 08/26/15 Pct Recovery = 109% Analysis Date = 08/21/15 Pct Recovery = 109% Analysis Date = 08/21/15 Pct Recovery = 109% Analysis Date = 08/17/15 Pct Recovery = 109% Analysis Date = 08/17/15 Pct Recovery = 109% Analysis Date = 08/12/15 Pct Recovery = 109% Analysis Date = 08/12/15 Pct Recovery = 109% Analysis Date = 08/07/15 Pct Recovery = 109% Analysis Date = 08/07/15 Pct Recovery = 109% Analysis Date = 08/02/15 Pct Recovery = 109% Analysis Date = 08/02/15 Pct Recovery = 109% Analysis Date = 07/29/15 Pct Recovery = 109% Analysis Date = 07/29/15 Pct Recovery = 109% Analysis Date = 07/24/15 Pct Recovery = 109% Analysis Date = 07/24/15 Pct Recovery = 109% Analysis Date = 07/19/15 Pct Recovery = 109% Analysis Date = 07/19/15 Pct Recovery = 109% Analysis Date = 07/14/15 Pct Recovery = 109% Analysis Date = 07/14/15 Pct Recovery = 109% Analysis Date = 07/09/15 Pct Recovery = 109% Analysis Date = 07/09/15 Pct Recovery = 109% Analysis Date = 07/05/15 Pct Recovery = 109% Analysis Date = 07/05/15 Pct Recovery = 109% Analysis Date = 06/30/15 Pct Recovery = 109% Analysis Date = 06/30/15 Pct Recovery = 109% Analysis Date = 06/25/15 Pct Recovery = 109% Analysis Date = 06/25/15 Pct Recovery = 109% Analysis Date = 06/20/15 Pct Recovery = 109% Analysis Date = 06/20/15 Pct Recovery = 109% Analysis Date = 06/16/15 Pct Recovery = 109% Analysis Date = 06/16/15 Pct Recovery = 109% Analysis Date = 06/11/15 Pct Recovery = 109% Analysis Date = 06/11/15 Pct Recovery = 109% Analysis Date = 06/06/15 Pct Recovery = 109% Analysis Date = 06/06/15 Pct Recovery = 109% Analysis Date = 06/01/15 Pct Recovery = 109% Analysis Date = 06/01/15 Pct Recovery = 109% Analysis Date = 05/27/15 Pct Recovery = 109% Analysis Date = 05/27/15 Pct Recovery = 109% Analysis Date = 05/23/15 Pct Recovery = 109% Analysis Date = 05/23/15 Pct Recovery = 109% Analysis Date = 05/18/15 Pct Recovery = 109% Analysis Date = 05/18/15 Pct Recovery = 109% Analysis Date = 05/13/15 Pct Recovery = 109% Analysis Date = 05/13/15 Pct Recovery = 109% Analysis Date = 05/08/15 Pct Recovery = 109% Analysis Date = 05/08/15 Pct Recovery = 109% Analysis Date = 05/04/15 Pct Recovery = 109% Analysis Date = 05/04/15 Pct Recovery = 109% Analysis Date = 04/29/15 Pct Recovery = 109% Analysis Date = 04/29/15 Pct Recovery = 109% Analysis Date = 04/24/15 Pct Recovery = 108% Analysis Date = 04/24/15 Pct Recovery = 108% Analysis Date = 04/19/15 Pct Recovery = 108% Analysis Date = 04/19/15 Pct Recovery = 108% Analysis Date = 04/14/15 Pct Recovery = 108% Analysis Date = 04/14/15 Pct Recovery = 108% Analysis Date = 04/10/15 Pct Recovery = 108% Analysis Date = 04/10/15 Pct Recovery = 108% Analysis Date = 04/05/15 Pct Recovery = 108% Analysis Date = 04/05/15 Pct Recovery = 108% Analysis Date = 03/31/15 Pct Recovery = 108% Analysis Date = 03/31/15 Pct Recovery = 108% Analysis Date = 03/26/15 Pct Recovery = 108% Analysis Date = 03/26/15 Pct Recovery = 108% Analysis Date = 03/22/15 Pct Recovery = 108% Analysis Date = 03/22/15 Pct Recovery = 108% Analysis Date = 03/17/15 Pct Recovery = 108% Analysis Date = 03/17/15 Pct Recovery = 108% Analysis Date = 03/12/15 Pct Recovery = 108% Analysis Date = 03/12/15 Pct Recovery = 108% Analysis Date = 03/07/15 Pct Recovery = 109% Analysis Date = 03/07/15 Pct Recovery = 109% Analysis Date = 03/02/15 Pct Recovery = 109% Analysis Date = 03/02/15 Pct Recovery = 109% Analysis Date = 02/26/15 Pct Recovery = 109% Analysis Date = 02/26/15 Pct Recovery = 109% Analysis Date = 02/21/15 Pct Recovery = 109% Analysis Date = 02/21/15 Pct Recovery = 109% Analysis Date = 02/16/15 Pct Recovery = 109% Analysis Date = 02/16/15 Pct Recovery = 109% Analysis Date = 02/11/15 Pct Recovery = 109% Analysis Date = 02/11/15 Pct Recovery = 109% Analysis Date = 02/07/15 Pct Recovery = 109% Analysis Date = 02/07/15 Pct Recovery = 109% Analysis Date = 02/02/15 Pct Recovery = 109% Analysis Date = 02/02/15 Pct Recovery = 109% Analysis Date = 01/28/15 Pct Recovery = 109% Analysis Date = 01/28/15 Pct Recovery = 109% Analysis Date = 01/23/15 Pct Recovery = 109% Analysis Date = 01/23/15 Pct Recovery = 109% Analysis Date = 01/18/15 Pct Recovery = 109% Analysis Date = 01/18/15 Pct Recovery = 109% Analysis Date = 01/14/15 Pct Recovery = 109% Analysis Date = 01/14/15 Pct Recovery = 109% Analysis Date = 01/09/15 Pct Recovery = 109% Analysis Date = 01/09/15 Pct Recovery = 109% Analysis Date = 01/04/15 Pct Recovery = 109% Analysis Date = 01/04/15 Pct Recovery = 109% Analysis Date = 12/30/14 Pct Recovery = 109% Analysis Date = 12/30/14 Pct Recovery = 109% Analysis Date = 12/25/14 Pct Recovery = 109% Analysis Date = 12/25/14 Pct Recovery = 109% Analysis Date = 12/21/14 Pct Recovery = 109% Analysis Date = 12/21/14 Pct Recovery = 109% Analysis Date = 12/16/14 Pct Recovery = 109% Analysis Date = 12/16/14 Pct Recovery = 109% Analysis Date = 12/11/14 Pct Recovery = 109% Analysis Date = 12/11/14 Pct Recovery = 109% Analysis Date = 12/06/14 Pct Recovery = 109% Analysis Date = 12/06/14 Pct Recovery = 109% Analysis Date = 12/02/14 Pct Recovery = 109% Analysis Date = 12/02/14 Pct Recovery = 109% Analysis Date = 11/27/14 Pct Recovery = 109% Analysis Date = 11/27/14 Pct Recovery = 109% Analysis Date = 11/22/14 Pct Recovery = 109% Analysis Date = 11/22/14 Pct Recovery = 109% Analysis Date = 11/17/14 Pct Recovery = 109% Analysis Date = 11/17/14 Pct Recovery = 109% Analysis Date = 11/12/14 Pct Recovery = 110% Analysis Date = 11/12/14 Pct Recovery = 110% Analysis Date = 11/08/14 Pct Recovery = 110% Analysis Date = 11/08/14 Pct Recovery = 110% Analysis Date = 11/03/14 Pct Recovery = 110% Analysis Date = 11/03/14 Pct Recovery = 110% Analysis Date = 10/29/14 Pct Recovery = 110% Analysis Date = 10/29/14 Pct Recovery = 110% Analysis Date = 10/24/14 Pct Recovery = 110% Analysis Date = 10/24/14 Pct Recovery = 110% Analysis Date = 10/20/14 Pct Recovery = 110% Analysis Date = 10/20/14 Pct Recovery = 110% Analysis Date = 10/15/14 Pct Recovery = 110% Analysis Date = 10/15/14 Pct Recovery = 110% Analysis Date = 10/10/14 Pct Recovery = 110% Analysis Date = 10/10/14 Pct Recovery = 110% Analysis Date = 10/05/14 Pct Recovery = 110% Analysis Date = 10/05/14 Pct Recovery = 110% Analysis Date = 09/30/14 Pct Recovery = 110% Analysis Date = 09/30/14 Pct Recovery = 110% Analysis Date = 09/26/14 Pct Recovery = 110% Analysis Date = 09/26/14 Pct Recovery = 110% Analysis Date = 09/21/14 Pct Recovery = 110% Analysis Date = 09/21/14 Pct Recovery = 110% Analysis Date = 09/16/14 Pct Recovery = 110% Analysis Date = 09/16/14 Pct Recovery = 110% Analysis Date = 09/11/14 Pct Recovery = 110% Analysis Date = 09/11/14 Pct Recovery = 110% Analysis Date = 09/07/14 Pct Recovery = 110% Analysis Date = 09/07/14 Pct Recovery = 110% Analysis Date = 09/02/14 Pct Recovery = 110% Analysis Date = 09/02/14 Pct Recovery = 110% Analysis Date = 08/28/14 Pct Recovery = 111% Analysis Date = 08/28/14 Pct Recovery = 111% Analysis Date = 08/23/14 Pct Recovery = 111% Analysis Date = 08/23/14 Pct Recovery = 111% Analysis Date = 08/18/14 Pct Recovery = 111% Analysis Date = 08/18/14 Pct Recovery = 111% Analysis Date = 08/14/14 Pct Recovery = 111% Analysis Date = 08/14/14 Pct Recovery = 111% Analysis Date = 08/09/14 Pct Recovery = 111% Analysis Date = 08/09/14 Pct Recovery = 111% Analysis Date = 08/04/14 Pct Recovery = 111% Analysis Date = 08/04/14 Pct Recovery = 111% Analysis Date = 07/30/14 Pct Recovery = 111% Analysis Date = 07/30/14 Pct Recovery = 111% Analysis Date = 07/26/14 Pct Recovery = 111% Analysis Date = 07/26/14 Pct Recovery = 111% Analysis Date = 07/21/14 Pct Recovery = 111% Analysis Date = 07/21/14 Pct Recovery = 111% Analysis Date = 07/16/14 Pct Recovery = 111% Analysis Date = 07/16/14 Pct Recovery = 111% Analysis Date = 07/11/14 Pct Recovery = 111% Analysis Date = 07/11/14 Pct Recovery = 111% Analysis Date = 07/06/14 Pct Recovery = 111% Analysis Date = 07/06/14 Pct Recovery = 111% Analysis Date = 07/02/14 Pct Recovery = 111% Analysis Date = 07/02/14 Pct Recovery = 111% Analysis Date = 06/27/14 Pct Recovery = 111% Analysis Date = 06/27/14 Pct Recovery = 111% Analysis Date = 06/22/14 Pct Recovery = 112% Analysis Date = 06/22/14 Pct Recovery = 112% Analysis Date = 06/17/14 Pct Recovery = 112% Analysis Date = 06/17/14 Pct Recovery = 112% Analysis Date = 06/13/14 Pct Recovery = 112% Analysis Date = 06/13/14 Pct Recovery = 112% Analysis Date = 06/08/14 Pct Recovery = 112% Analysis Date = 06/08/14 Pct Recovery = 112% Analysis Date = 06/03/14 Pct Recovery = 112% Analysis Date = 06/03/14 Pct Recovery = 112% Analysis Date = 05/29/14 Pct Recovery = 112% Analysis Date = 05/29/14 Pct Recovery = 112% Analysis Date = 05/24/14 Pct Recovery = 112% Analysis Date = 05/24/14 Pct Recovery = 112% Analysis Date = 05/20/14 Pct Recovery = 112% Analysis Date = 05/20/14 Pct Recovery = 112% Analysis Date = 05/15/14 Pct Recovery = 112% Analysis Date = 05/15/14 Pct Recovery = 112% Analysis Date = 05/10/14 Pct Recovery = 113% Analysis Date = 05/10/14 Pct Recovery = 113% Analysis Date = 05/05/14 Pct Recovery = 113% Analysis Date = 05/05/14 Pct Recovery = 113% Analysis Date = 05/01/14 Pct Recovery = 113% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
2,2-DICHLORO-1,1,1-TRIFLUOROETHANE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 42 106% 12% 108% 9%
Total 42 106% 12% 108% 9%

Sample Statistics
2,2-DICHLORO-1,1,1-TRIFLUOROETHANE

Characteristic N % % Basis
Plotted 42 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 42 .  
False Negatives 0 0% 0 out of 42
Not Spiked 31 .  
False Positives 0 0% 0 out of 31

BQS OBSP Determination:
2,2-DICHLOROPROPANE
METHOD: 4440 , TESTIDCODE: 77170GCM66
Open Data Set

Analysis Date = 12/16/16 SpikeMix = NSI 041816AVOC: 40 µl & ChemService 5082900: 40 µl Pct Recovery = 96% Analysis Date = 08/04/16 SpikeMix = Crescent 03FF058: 40 µl & Supelco LC20141V: 40 µl Pct Recovery = 80% Analysis Date = 07/20/16 SpikeMix = Supelco LC20141V: 40 µl & Accu 216041125: 40 µl Pct Recovery = 95% Analysis Date = 08/26/16 SpikeMix = NSI 041816AVOC: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 85% Analysis Date = 08/12/16 SpikeMix = ChemService 5082900: 25 µl & Phenova B20160319: 25 µl Pct Recovery = 93% Analysis Date = 06/30/16 SpikeMix = Crescent 03FF058: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 82% Analysis Date = 11/21/16 SpikeMix = Crescent 03FF058: 25 µl & Supelco LC20141V: 25 µl Pct Recovery = 82% Analysis Date = 09/08/16 SpikeMix = Supelco LC20141V: 25 µl & Accu 216041125: 25 µl Pct Recovery = 76% Analysis Date = 03/06/15 SpikeMix = ERA 0227-14-06.1A: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 62% Analysis Date = 12/17/14 SpikeMix = Supelco LC06438: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 74% Analysis Date = 09/21/14 SpikeMix = Supelco LC06438: 20 µl Pct Recovery = 72% Analysis Date = 06/10/14 SpikeMix = NSI 032614: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 85% Analysis Date = 03/19/15 SpikeMix = Spex Organics C1140417015: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 92% Analysis Date = 11/22/14 SpikeMix = NSI 032614: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 90% Analysis Date = 08/19/14 SpikeMix = Spex Organics C1140417015: 20 µl & Accu 214031115: 20 µl Pct Recovery = 88% Analysis Date = 08/16/14 SpikeMix = ERA 0227-14-06.1A: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 82% Analysis Date = 09/29/15 SpikeMix = Accu 215041380: 25 µl & ERA 0406-15-03: 25 µl Pct Recovery = 60% Analysis Date = 06/16/15 SpikeMix = ERA 0406-15-03: 25 µl & Supelco LC13545: 25 µl Pct Recovery = 57% Analysis Date = 07/13/15 SpikeMix = Crescent 04EE008: 25 µl & NSI 050515AVOC: 25 µl Pct Recovery = 58% Analysis Date = 11/29/16 SpikeMix = ChemService 5082900: 15 µl & Phenova B20160319: 15 µl Pct Recovery = 85% Analysis Date = 09/28/16 SpikeMix = Crescent 03FF058: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 79% Analysis Date = 06/30/16 SpikeMix = ChemService 5082900: 15 µl & Accu 216041125: 15 µl Pct Recovery = 97% Analysis Date = 06/15/16 SpikeMix = NSI 041816AVOC: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 67% Analysis Date = 10/13/16 SpikeMix = NSI 041816AVOC: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 100% Analysis Date = 05/27/16 SpikeMix = Phenova B20160319: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 107% Analysis Date = 04/26/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 62% Analysis Date = 03/04/16 SpikeMix = Accu 215041380: 15 µl & ERA 0406-15-03: 15 µl Pct Recovery = 102% Analysis Date = 02/05/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 68% Analysis Date = 10/16/15 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 72% Analysis Date = 11/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 83% Analysis Date = 10/17/15 SpikeMix = Crescent 04EE008: 15 µl & NSI 050515AVOC: 15 µl Pct Recovery = 76% Analysis Date = 06/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Accu 215041380: 15 µl Pct Recovery = 70% Analysis Date = 10/21/14 SpikeMix = ERA 0227-14-06.1A: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 90% Analysis Date = 06/18/14 SpikeMix = Supelco LC06438: 10 µl & Accu 214031115: 10 µl Pct Recovery = 94% Analysis Date = 05/30/14 SpikeMix = NSI 032614: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 67% Analysis Date = 05/03/14 SpikeMix = Crescent 03DD004: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 87% Analysis Date = 11/06/14 SpikeMix = Spex Organics C1140417015: 10 µl & Crescent 03DD004: 10 µl Pct Recovery = 79% Analysis Date = 09/09/14 SpikeMix = NSI 032614: 10 µl & Spex Organics C1140417015: 10 µl Pct Recovery = 84% Analysis Date = 07/23/14 SpikeMix = Spex Organics C1140417015: 10 µl & Accu 214031115: 10 µl Pct Recovery = 93% Analysis Date = 07/11/14 SpikeMix = Spex Organics C1140417015: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 74% Analysis Date = 11/20/15 SpikeMix = Accu 215041380: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 83% Analysis Date = 08/07/15 SpikeMix = Crescent 04EE008: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 65% Analysis Date = 06/27/15 SpikeMix = ERA 0406-15-03: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 78% Analysis Date = 03/17/16 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 103% Analysis Date = 01/27/16 SpikeMix = Crescent 04EE008: 10 µl & NSI 050515AVOC: 10 µl Pct Recovery = 73% Analysis Date = 12/10/15 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 87% Analysis Date = 09/03/15 SpikeMix = NSI 050515AVOC: 10 µl & Spex Organics EN150428007: 10 µl Pct Recovery = 69% Analysis Date = 12/16/16 Pct Recovery = 89% Analysis Date = 12/11/16 Pct Recovery = 88% Analysis Date = 12/11/16 Pct Recovery = 88% Analysis Date = 12/06/16 Pct Recovery = 88% Analysis Date = 12/06/16 Pct Recovery = 88% Analysis Date = 12/01/16 Pct Recovery = 88% Analysis Date = 12/01/16 Pct Recovery = 88% Analysis Date = 11/26/16 Pct Recovery = 88% Analysis Date = 11/26/16 Pct Recovery = 88% Analysis Date = 11/22/16 Pct Recovery = 88% Analysis Date = 11/22/16 Pct Recovery = 88% Analysis Date = 11/17/16 Pct Recovery = 88% Analysis Date = 11/17/16 Pct Recovery = 88% Analysis Date = 11/12/16 Pct Recovery = 88% Analysis Date = 11/12/16 Pct Recovery = 88% Analysis Date = 11/07/16 Pct Recovery = 88% Analysis Date = 11/07/16 Pct Recovery = 88% Analysis Date = 11/02/16 Pct Recovery = 88% Analysis Date = 11/02/16 Pct Recovery = 88% Analysis Date = 10/29/16 Pct Recovery = 88% Analysis Date = 10/29/16 Pct Recovery = 88% Analysis Date = 10/24/16 Pct Recovery = 88% Analysis Date = 10/24/16 Pct Recovery = 88% Analysis Date = 10/19/16 Pct Recovery = 88% Analysis Date = 10/19/16 Pct Recovery = 88% Analysis Date = 10/14/16 Pct Recovery = 88% Analysis Date = 10/14/16 Pct Recovery = 88% Analysis Date = 10/09/16 Pct Recovery = 87% Analysis Date = 10/09/16 Pct Recovery = 87% Analysis Date = 10/05/16 Pct Recovery = 87% Analysis Date = 10/05/16 Pct Recovery = 87% Analysis Date = 09/30/16 Pct Recovery = 87% Analysis Date = 09/30/16 Pct Recovery = 87% Analysis Date = 09/25/16 Pct Recovery = 87% Analysis Date = 09/25/16 Pct Recovery = 87% Analysis Date = 09/20/16 Pct Recovery = 87% Analysis Date = 09/20/16 Pct Recovery = 87% Analysis Date = 09/15/16 Pct Recovery = 87% Analysis Date = 09/15/16 Pct Recovery = 87% Analysis Date = 09/11/16 Pct Recovery = 87% Analysis Date = 09/11/16 Pct Recovery = 87% Analysis Date = 09/06/16 Pct Recovery = 87% Analysis Date = 09/06/16 Pct Recovery = 87% Analysis Date = 09/01/16 Pct Recovery = 87% Analysis Date = 09/01/16 Pct Recovery = 87% Analysis Date = 08/27/16 Pct Recovery = 87% Analysis Date = 08/27/16 Pct Recovery = 87% Analysis Date = 08/23/16 Pct Recovery = 87% Analysis Date = 08/23/16 Pct Recovery = 87% Analysis Date = 08/18/16 Pct Recovery = 87% Analysis Date = 08/18/16 Pct Recovery = 87% Analysis Date = 08/13/16 Pct Recovery = 86% Analysis Date = 08/13/16 Pct Recovery = 86% Analysis Date = 08/08/16 Pct Recovery = 86% Analysis Date = 08/08/16 Pct Recovery = 86% Analysis Date = 08/03/16 Pct Recovery = 86% Analysis Date = 08/03/16 Pct Recovery = 86% Analysis Date = 07/30/16 Pct Recovery = 86% Analysis Date = 07/30/16 Pct Recovery = 86% Analysis Date = 07/25/16 Pct Recovery = 86% Analysis Date = 07/25/16 Pct Recovery = 86% Analysis Date = 07/20/16 Pct Recovery = 86% Analysis Date = 07/20/16 Pct Recovery = 86% Analysis Date = 07/15/16 Pct Recovery = 86% Analysis Date = 07/15/16 Pct Recovery = 86% Analysis Date = 07/10/16 Pct Recovery = 86% Analysis Date = 07/10/16 Pct Recovery = 86% Analysis Date = 07/06/16 Pct Recovery = 86% Analysis Date = 07/06/16 Pct Recovery = 86% Analysis Date = 07/01/16 Pct Recovery = 86% Analysis Date = 07/01/16 Pct Recovery = 86% Analysis Date = 06/26/16 Pct Recovery = 86% Analysis Date = 06/26/16 Pct Recovery = 86% Analysis Date = 06/21/16 Pct Recovery = 85% Analysis Date = 06/21/16 Pct Recovery = 85% Analysis Date = 06/16/16 Pct Recovery = 85% Analysis Date = 06/16/16 Pct Recovery = 85% Analysis Date = 06/12/16 Pct Recovery = 85% Analysis Date = 06/12/16 Pct Recovery = 85% Analysis Date = 06/07/16 Pct Recovery = 85% Analysis Date = 06/07/16 Pct Recovery = 85% Analysis Date = 06/02/16 Pct Recovery = 85% Analysis Date = 06/02/16 Pct Recovery = 85% Analysis Date = 05/28/16 Pct Recovery = 85% Analysis Date = 05/28/16 Pct Recovery = 85% Analysis Date = 05/24/16 Pct Recovery = 85% Analysis Date = 05/24/16 Pct Recovery = 85% Analysis Date = 05/19/16 Pct Recovery = 85% Analysis Date = 05/19/16 Pct Recovery = 85% Analysis Date = 05/14/16 Pct Recovery = 85% Analysis Date = 05/14/16 Pct Recovery = 85% Analysis Date = 05/09/16 Pct Recovery = 84% Analysis Date = 05/09/16 Pct Recovery = 84% Analysis Date = 05/04/16 Pct Recovery = 84% Analysis Date = 05/04/16 Pct Recovery = 84% Analysis Date = 04/30/16 Pct Recovery = 84% Analysis Date = 04/30/16 Pct Recovery = 84% Analysis Date = 04/25/16 Pct Recovery = 84% Analysis Date = 04/25/16 Pct Recovery = 84% Analysis Date = 04/20/16 Pct Recovery = 84% Analysis Date = 04/20/16 Pct Recovery = 84% Analysis Date = 04/15/16 Pct Recovery = 84% Analysis Date = 04/15/16 Pct Recovery = 84% Analysis Date = 04/10/16 Pct Recovery = 84% Analysis Date = 04/10/16 Pct Recovery = 84% Analysis Date = 04/06/16 Pct Recovery = 83% Analysis Date = 04/06/16 Pct Recovery = 83% Analysis Date = 04/01/16 Pct Recovery = 83% Analysis Date = 04/01/16 Pct Recovery = 83% Analysis Date = 03/27/16 Pct Recovery = 83% Analysis Date = 03/27/16 Pct Recovery = 83% Analysis Date = 03/22/16 Pct Recovery = 83% Analysis Date = 03/22/16 Pct Recovery = 83% Analysis Date = 03/17/16 Pct Recovery = 83% Analysis Date = 03/17/16 Pct Recovery = 83% Analysis Date = 03/13/16 Pct Recovery = 83% Analysis Date = 03/13/16 Pct Recovery = 83% Analysis Date = 03/08/16 Pct Recovery = 82% Analysis Date = 03/08/16 Pct Recovery = 82% Analysis Date = 03/03/16 Pct Recovery = 82% Analysis Date = 03/03/16 Pct Recovery = 82% Analysis Date = 02/27/16 Pct Recovery = 82% Analysis Date = 02/27/16 Pct Recovery = 82% Analysis Date = 02/23/16 Pct Recovery = 82% Analysis Date = 02/23/16 Pct Recovery = 82% Analysis Date = 02/18/16 Pct Recovery = 82% Analysis Date = 02/18/16 Pct Recovery = 82% Analysis Date = 02/13/16 Pct Recovery = 82% Analysis Date = 02/13/16 Pct Recovery = 82% Analysis Date = 02/08/16 Pct Recovery = 81% Analysis Date = 02/08/16 Pct Recovery = 81% Analysis Date = 02/03/16 Pct Recovery = 81% Analysis Date = 02/03/16 Pct Recovery = 81% Analysis Date = 01/30/16 Pct Recovery = 81% Analysis Date = 01/30/16 Pct Recovery = 81% Analysis Date = 01/25/16 Pct Recovery = 81% Analysis Date = 01/25/16 Pct Recovery = 81% Analysis Date = 01/20/16 Pct Recovery = 80% Analysis Date = 01/20/16 Pct Recovery = 80% Analysis Date = 01/15/16 Pct Recovery = 80% Analysis Date = 01/15/16 Pct Recovery = 80% Analysis Date = 01/10/16 Pct Recovery = 80% Analysis Date = 01/10/16 Pct Recovery = 80% Analysis Date = 01/06/16 Pct Recovery = 79% Analysis Date = 01/06/16 Pct Recovery = 79% Analysis Date = 01/01/16 Pct Recovery = 79% Analysis Date = 01/01/16 Pct Recovery = 79% Analysis Date = 12/27/15 Pct Recovery = 79% Analysis Date = 12/27/15 Pct Recovery = 79% Analysis Date = 12/22/15 Pct Recovery = 79% Analysis Date = 12/22/15 Pct Recovery = 79% Analysis Date = 12/17/15 Pct Recovery = 78% Analysis Date = 12/17/15 Pct Recovery = 78% Analysis Date = 12/13/15 Pct Recovery = 78% Analysis Date = 12/13/15 Pct Recovery = 78% Analysis Date = 12/08/15 Pct Recovery = 78% Analysis Date = 12/08/15 Pct Recovery = 78% Analysis Date = 12/03/15 Pct Recovery = 77% Analysis Date = 12/03/15 Pct Recovery = 77% Analysis Date = 11/28/15 Pct Recovery = 77% Analysis Date = 11/28/15 Pct Recovery = 77% Analysis Date = 11/24/15 Pct Recovery = 77% Analysis Date = 11/24/15 Pct Recovery = 77% Analysis Date = 11/19/15 Pct Recovery = 76% Analysis Date = 11/19/15 Pct Recovery = 76% Analysis Date = 11/14/15 Pct Recovery = 76% Analysis Date = 11/14/15 Pct Recovery = 76% Analysis Date = 11/09/15 Pct Recovery = 76% Analysis Date = 11/09/15 Pct Recovery = 76% Analysis Date = 11/04/15 Pct Recovery = 76% Analysis Date = 11/04/15 Pct Recovery = 76% Analysis Date = 10/31/15 Pct Recovery = 75% Analysis Date = 10/31/15 Pct Recovery = 75% Analysis Date = 10/26/15 Pct Recovery = 75% Analysis Date = 10/26/15 Pct Recovery = 75% Analysis Date = 10/21/15 Pct Recovery = 75% Analysis Date = 10/21/15 Pct Recovery = 75% Analysis Date = 10/16/15 Pct Recovery = 75% Analysis Date = 10/16/15 Pct Recovery = 75% Analysis Date = 10/11/15 Pct Recovery = 75% Analysis Date = 10/11/15 Pct Recovery = 75% Analysis Date = 10/07/15 Pct Recovery = 74% Analysis Date = 10/07/15 Pct Recovery = 74% Analysis Date = 10/02/15 Pct Recovery = 74% Analysis Date = 10/02/15 Pct Recovery = 74% Analysis Date = 09/27/15 Pct Recovery = 74% Analysis Date = 09/27/15 Pct Recovery = 74% Analysis Date = 09/22/15 Pct Recovery = 74% Analysis Date = 09/22/15 Pct Recovery = 74% Analysis Date = 09/17/15 Pct Recovery = 74% Analysis Date = 09/17/15 Pct Recovery = 74% Analysis Date = 09/13/15 Pct Recovery = 74% Analysis Date = 09/13/15 Pct Recovery = 74% Analysis Date = 09/08/15 Pct Recovery = 74% Analysis Date = 09/08/15 Pct Recovery = 74% Analysis Date = 09/03/15 Pct Recovery = 74% Analysis Date = 09/03/15 Pct Recovery = 74% Analysis Date = 08/29/15 Pct Recovery = 73% Analysis Date = 08/29/15 Pct Recovery = 73% Analysis Date = 08/25/15 Pct Recovery = 73% Analysis Date = 08/25/15 Pct Recovery = 73% Analysis Date = 08/20/15 Pct Recovery = 73% Analysis Date = 08/20/15 Pct Recovery = 73% Analysis Date = 08/15/15 Pct Recovery = 73% Analysis Date = 08/15/15 Pct Recovery = 73% Analysis Date = 08/10/15 Pct Recovery = 73% Analysis Date = 08/10/15 Pct Recovery = 73% Analysis Date = 08/05/15 Pct Recovery = 73% Analysis Date = 08/05/15 Pct Recovery = 73% Analysis Date = 08/01/15 Pct Recovery = 73% Analysis Date = 08/01/15 Pct Recovery = 73% Analysis Date = 07/27/15 Pct Recovery = 73% Analysis Date = 07/27/15 Pct Recovery = 73% Analysis Date = 07/22/15 Pct Recovery = 73% Analysis Date = 07/22/15 Pct Recovery = 73% Analysis Date = 07/17/15 Pct Recovery = 73% Analysis Date = 07/17/15 Pct Recovery = 73% Analysis Date = 07/12/15 Pct Recovery = 73% Analysis Date = 07/12/15 Pct Recovery = 73% Analysis Date = 07/08/15 Pct Recovery = 73% Analysis Date = 07/08/15 Pct Recovery = 73% Analysis Date = 07/03/15 Pct Recovery = 73% Analysis Date = 07/03/15 Pct Recovery = 73% Analysis Date = 06/28/15 Pct Recovery = 73% Analysis Date = 06/28/15 Pct Recovery = 73% Analysis Date = 06/23/15 Pct Recovery = 73% Analysis Date = 06/23/15 Pct Recovery = 73% Analysis Date = 06/18/15 Pct Recovery = 73% Analysis Date = 06/18/15 Pct Recovery = 73% Analysis Date = 06/14/15 Pct Recovery = 73% Analysis Date = 06/14/15 Pct Recovery = 73% Analysis Date = 06/09/15 Pct Recovery = 73% Analysis Date = 06/09/15 Pct Recovery = 73% Analysis Date = 06/04/15 Pct Recovery = 73% Analysis Date = 06/04/15 Pct Recovery = 73% Analysis Date = 05/30/15 Pct Recovery = 73% Analysis Date = 05/30/15 Pct Recovery = 73% Analysis Date = 05/25/15 Pct Recovery = 73% Analysis Date = 05/25/15 Pct Recovery = 73% Analysis Date = 05/21/15 Pct Recovery = 74% Analysis Date = 05/21/15 Pct Recovery = 74% Analysis Date = 05/16/15 Pct Recovery = 74% Analysis Date = 05/16/15 Pct Recovery = 74% Analysis Date = 05/11/15 Pct Recovery = 74% Analysis Date = 05/11/15 Pct Recovery = 74% Analysis Date = 05/06/15 Pct Recovery = 74% Analysis Date = 05/06/15 Pct Recovery = 74% Analysis Date = 05/02/15 Pct Recovery = 74% Analysis Date = 05/02/15 Pct Recovery = 74% Analysis Date = 04/27/15 Pct Recovery = 74% Analysis Date = 04/27/15 Pct Recovery = 74% Analysis Date = 04/22/15 Pct Recovery = 74% Analysis Date = 04/22/15 Pct Recovery = 74% Analysis Date = 04/17/15 Pct Recovery = 74% Analysis Date = 04/17/15 Pct Recovery = 74% Analysis Date = 04/12/15 Pct Recovery = 74% Analysis Date = 04/12/15 Pct Recovery = 74% Analysis Date = 04/08/15 Pct Recovery = 74% Analysis Date = 04/08/15 Pct Recovery = 74% Analysis Date = 04/03/15 Pct Recovery = 74% Analysis Date = 04/03/15 Pct Recovery = 74% Analysis Date = 03/29/15 Pct Recovery = 75% Analysis Date = 03/29/15 Pct Recovery = 75% Analysis Date = 03/24/15 Pct Recovery = 75% Analysis Date = 03/24/15 Pct Recovery = 75% Analysis Date = 03/19/15 Pct Recovery = 75% Analysis Date = 03/19/15 Pct Recovery = 75% Analysis Date = 03/15/15 Pct Recovery = 75% Analysis Date = 03/15/15 Pct Recovery = 75% Analysis Date = 03/10/15 Pct Recovery = 75% Analysis Date = 03/10/15 Pct Recovery = 75% Analysis Date = 03/05/15 Pct Recovery = 75% Analysis Date = 03/05/15 Pct Recovery = 75% Analysis Date = 02/28/15 Pct Recovery = 75% Analysis Date = 02/28/15 Pct Recovery = 75% Analysis Date = 02/23/15 Pct Recovery = 75% Analysis Date = 02/23/15 Pct Recovery = 75% Analysis Date = 02/19/15 Pct Recovery = 76% Analysis Date = 02/19/15 Pct Recovery = 76% Analysis Date = 02/14/15 Pct Recovery = 76% Analysis Date = 02/14/15 Pct Recovery = 76% Analysis Date = 02/09/15 Pct Recovery = 76% Analysis Date = 02/09/15 Pct Recovery = 76% Analysis Date = 02/04/15 Pct Recovery = 76% Analysis Date = 02/04/15 Pct Recovery = 76% Analysis Date = 01/31/15 Pct Recovery = 76% Analysis Date = 01/31/15 Pct Recovery = 76% Analysis Date = 01/26/15 Pct Recovery = 76% Analysis Date = 01/26/15 Pct Recovery = 76% Analysis Date = 01/21/15 Pct Recovery = 77% Analysis Date = 01/21/15 Pct Recovery = 77% Analysis Date = 01/16/15 Pct Recovery = 77% Analysis Date = 01/16/15 Pct Recovery = 77% Analysis Date = 01/11/15 Pct Recovery = 77% Analysis Date = 01/11/15 Pct Recovery = 77% Analysis Date = 01/07/15 Pct Recovery = 77% Analysis Date = 01/07/15 Pct Recovery = 77% Analysis Date = 01/02/15 Pct Recovery = 77% Analysis Date = 01/02/15 Pct Recovery = 77% Analysis Date = 12/28/14 Pct Recovery = 78% Analysis Date = 12/28/14 Pct Recovery = 78% Analysis Date = 12/23/14 Pct Recovery = 78% Analysis Date = 12/23/14 Pct Recovery = 78% Analysis Date = 12/18/14 Pct Recovery = 78% Analysis Date = 12/18/14 Pct Recovery = 78% Analysis Date = 12/14/14 Pct Recovery = 78% Analysis Date = 12/14/14 Pct Recovery = 78% Analysis Date = 12/09/14 Pct Recovery = 78% Analysis Date = 12/09/14 Pct Recovery = 78% Analysis Date = 12/04/14 Pct Recovery = 78% Analysis Date = 12/04/14 Pct Recovery = 78% Analysis Date = 11/29/14 Pct Recovery = 79% Analysis Date = 11/29/14 Pct Recovery = 79% Analysis Date = 11/24/14 Pct Recovery = 79% Analysis Date = 11/24/14 Pct Recovery = 79% Analysis Date = 11/20/14 Pct Recovery = 79% Analysis Date = 11/20/14 Pct Recovery = 79% Analysis Date = 11/15/14 Pct Recovery = 79% Analysis Date = 11/15/14 Pct Recovery = 79% Analysis Date = 11/10/14 Pct Recovery = 79% Analysis Date = 11/10/14 Pct Recovery = 79% Analysis Date = 11/05/14 Pct Recovery = 80% Analysis Date = 11/05/14 Pct Recovery = 80% Analysis Date = 11/01/14 Pct Recovery = 80% Analysis Date = 11/01/14 Pct Recovery = 80% Analysis Date = 10/27/14 Pct Recovery = 80% Analysis Date = 10/27/14 Pct Recovery = 80% Analysis Date = 10/22/14 Pct Recovery = 80% Analysis Date = 10/22/14 Pct Recovery = 80% Analysis Date = 10/17/14 Pct Recovery = 80% Analysis Date = 10/17/14 Pct Recovery = 80% Analysis Date = 10/12/14 Pct Recovery = 80% Analysis Date = 10/12/14 Pct Recovery = 80% Analysis Date = 10/08/14 Pct Recovery = 81% Analysis Date = 10/08/14 Pct Recovery = 81% Analysis Date = 10/03/14 Pct Recovery = 81% Analysis Date = 10/03/14 Pct Recovery = 81% Analysis Date = 09/28/14 Pct Recovery = 81% Analysis Date = 09/28/14 Pct Recovery = 81% Analysis Date = 09/23/14 Pct Recovery = 81% Analysis Date = 09/23/14 Pct Recovery = 81% Analysis Date = 09/18/14 Pct Recovery = 81% Analysis Date = 09/18/14 Pct Recovery = 81% Analysis Date = 09/14/14 Pct Recovery = 82% Analysis Date = 09/14/14 Pct Recovery = 82% Analysis Date = 09/09/14 Pct Recovery = 82% Analysis Date = 09/09/14 Pct Recovery = 82% Analysis Date = 09/04/14 Pct Recovery = 82% Analysis Date = 09/04/14 Pct Recovery = 82% Analysis Date = 08/30/14 Pct Recovery = 82% Analysis Date = 08/30/14 Pct Recovery = 82% Analysis Date = 08/25/14 Pct Recovery = 82% Analysis Date = 08/25/14 Pct Recovery = 82% Analysis Date = 08/21/14 Pct Recovery = 82% Analysis Date = 08/21/14 Pct Recovery = 82% Analysis Date = 08/16/14 Pct Recovery = 83% Analysis Date = 08/16/14 Pct Recovery = 83% Analysis Date = 08/11/14 Pct Recovery = 83% Analysis Date = 08/11/14 Pct Recovery = 83% Analysis Date = 08/06/14 Pct Recovery = 83% Analysis Date = 08/06/14 Pct Recovery = 83% Analysis Date = 08/02/14 Pct Recovery = 83% Analysis Date = 08/02/14 Pct Recovery = 83% Analysis Date = 07/28/14 Pct Recovery = 83% Analysis Date = 07/28/14 Pct Recovery = 83% Analysis Date = 07/23/14 Pct Recovery = 83% Analysis Date = 07/23/14 Pct Recovery = 83% Analysis Date = 07/18/14 Pct Recovery = 84% Analysis Date = 07/18/14 Pct Recovery = 84% Analysis Date = 07/13/14 Pct Recovery = 84% Analysis Date = 07/13/14 Pct Recovery = 84% Analysis Date = 07/09/14 Pct Recovery = 84% Analysis Date = 07/09/14 Pct Recovery = 84% Analysis Date = 07/04/14 Pct Recovery = 84% Analysis Date = 07/04/14 Pct Recovery = 84% Analysis Date = 06/29/14 Pct Recovery = 84% Analysis Date = 06/29/14 Pct Recovery = 84% Analysis Date = 06/24/14 Pct Recovery = 84% Analysis Date = 06/24/14 Pct Recovery = 84% Analysis Date = 06/19/14 Pct Recovery = 85% Analysis Date = 06/19/14 Pct Recovery = 85% Analysis Date = 06/15/14 Pct Recovery = 85% Analysis Date = 06/15/14 Pct Recovery = 85% Analysis Date = 06/10/14 Pct Recovery = 85% Analysis Date = 06/10/14 Pct Recovery = 85% Analysis Date = 06/05/14 Pct Recovery = 85% Analysis Date = 06/05/14 Pct Recovery = 85% Analysis Date = 05/31/14 Pct Recovery = 85% Analysis Date = 05/31/14 Pct Recovery = 85% Analysis Date = 05/26/14 Pct Recovery = 85% Analysis Date = 05/26/14 Pct Recovery = 85% Analysis Date = 05/22/14 Pct Recovery = 86% Analysis Date = 05/22/14 Pct Recovery = 86% Analysis Date = 05/17/14 Pct Recovery = 86% Analysis Date = 05/17/14 Pct Recovery = 86% Analysis Date = 05/12/14 Pct Recovery = 86% Analysis Date = 05/12/14 Pct Recovery = 86% Analysis Date = 05/07/14 Pct Recovery = 86% Analysis Date = 05/07/14 Pct Recovery = 86% Analysis Date = 05/03/14 Pct Recovery = 86% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
2,2-DICHLOROPROPANE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 47 81% 13% 82% 13%
Total 47 81% 13% 82% 13%

Sample Statistics
2,2-DICHLOROPROPANE

Characteristic N % % Basis
Plotted 47 100% Spiked
Estimated Values 3 6% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 47 .  
False Negatives 0 0% 0 out of 47
Not Spiked 26 .  
False Positives 0 0% 0 out of 26

BQS OBSP Determination:
2-BUTANONE
METHOD: 4440 , TESTIDCODE: 81595GCM66
Open Data Set

Analysis Date = 12/12/16 SpikeMix = Accu 216041125: 40 µl & Crescent 03FF058: 40 µl Pct Recovery = 107% Analysis Date = 07/20/16 SpikeMix = Supelco LC20141V: 40 µl & Accu 216041125: 40 µl Pct Recovery = 103% Analysis Date = 07/14/16 SpikeMix = Accu 216041125: 40 µl & NSI 041816AVOC: 40 µl Pct Recovery = 83% Analysis Date = 08/12/16 SpikeMix = ChemService 5082900: 25 µl & Phenova B20160319: 25 µl Pct Recovery = 93% Analysis Date = 06/21/16 SpikeMix = Phenova B20160319: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 99% Analysis Date = 09/08/16 SpikeMix = Supelco LC20141V: 25 µl & Accu 216041125: 25 µl Pct Recovery = 71% Analysis Date = 05/24/16 SpikeMix = Accu 216041125: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 97% Analysis Date = 09/29/15 SpikeMix = Accu 215041380: 25 µl & ERA 0406-15-03: 25 µl Pct Recovery = 85% Analysis Date = 08/15/15 SpikeMix = Supelco LC13545: 25 µl & Crescent 04EE008: 25 µl Pct Recovery = 100% Analysis Date = 07/13/15 SpikeMix = Crescent 04EE008: 25 µl & NSI 050515AVOC: 25 µl Pct Recovery = 94% Analysis Date = 11/22/14 SpikeMix = NSI 032614: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 89% Analysis Date = 06/10/14 SpikeMix = Crescent 03DD004: 20 µl & NSI 032614: 20 µl Pct Recovery = 108% Analysis Date = 06/10/14 SpikeMix = NSI 032614: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 120% Analysis Date = 05/01/14 SpikeMix = Accu 214031115: 20 µl & NSI 032614: 20 µl Pct Recovery = 90% Analysis Date = 04/09/15 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 90% Analysis Date = 03/06/15 SpikeMix = ERA 0227-14-06.1A: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 114% Analysis Date = 11/14/14 SpikeMix = Crescent 03DD004: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 92% Analysis Date = 08/16/14 SpikeMix = ERA 0227-14-06.1A: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 86% Analysis Date = 07/01/14 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 94% Analysis Date = 11/29/16 SpikeMix = ChemService 5082900: 15 µl & Phenova B20160319: 15 µl Pct Recovery = 97% Analysis Date = 09/08/16 SpikeMix = Phenova B20160319: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 81% Analysis Date = 07/29/16 SpikeMix = Phenova B20160319: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 90% Analysis Date = 05/27/16 SpikeMix = Phenova B20160319: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 88% Analysis Date = 10/13/16 SpikeMix = Accu 216041125: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 96% Analysis Date = 08/20/16 SpikeMix = Accu 216041125: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 111% Analysis Date = 06/30/16 SpikeMix = ChemService 5082900: 15 µl & Accu 216041125: 15 µl Pct Recovery = 61% Analysis Date = 04/02/16 SpikeMix = Supelco LC13545: 15 µl & Accu 215041380: 15 µl Pct Recovery = 79% Analysis Date = 03/04/16 SpikeMix = Accu 215041380: 15 µl & ERA 0406-15-03: 15 µl Pct Recovery = 87% Analysis Date = 06/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Accu 215041380: 15 µl Pct Recovery = 77% Analysis Date = 12/18/15 SpikeMix = Supelco LC13545: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 104% Analysis Date = 10/17/15 SpikeMix = Crescent 04EE008: 15 µl & NSI 050515AVOC: 15 µl Pct Recovery = 97% Analysis Date = 05/09/15 SpikeMix = Spex Organics EN150428007: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 106% Analysis Date = 09/09/14 SpikeMix = Accu 214031115: 10 µl & NSI 032614: 10 µl Pct Recovery = 113% Analysis Date = 09/09/14 SpikeMix = NSI 032614: 10 µl & Spex Organics C1140417015: 10 µl Pct Recovery = 103% Analysis Date = 07/29/14 SpikeMix = Crescent 03DD004: 10 µl & NSI 032614: 10 µl Pct Recovery = 94% Analysis Date = 05/30/14 SpikeMix = NSI 032614: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 115% Analysis Date = 01/13/15 SpikeMix = Accu 214031115: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 95% Analysis Date = 10/21/14 SpikeMix = ERA 0227-14-06.1A: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 90% Analysis Date = 10/04/14 SpikeMix = Crescent 03DD004: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 76% Analysis Date = 07/11/14 SpikeMix = Spex Organics C1140417015: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 105% Analysis Date = 02/18/16 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 82% Analysis Date = 11/20/15 SpikeMix = Accu 215041380: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 85% Analysis Date = 11/12/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 84% Analysis Date = 05/21/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 102% Analysis Date = 05/13/16 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 90% Analysis Date = 01/27/16 SpikeMix = Crescent 04EE008: 10 µl & NSI 050515AVOC: 10 µl Pct Recovery = 87% Analysis Date = 07/31/15 SpikeMix = Crescent 04EE008: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 110% Analysis Date = 05/09/15 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 87% Analysis Date = 12/11/16 Pct Recovery = 94% Analysis Date = 12/07/16 Pct Recovery = 94% Analysis Date = 12/07/16 Pct Recovery = 94% Analysis Date = 12/02/16 Pct Recovery = 94% Analysis Date = 12/02/16 Pct Recovery = 94% Analysis Date = 11/27/16 Pct Recovery = 94% Analysis Date = 11/27/16 Pct Recovery = 94% Analysis Date = 11/22/16 Pct Recovery = 94% Analysis Date = 11/22/16 Pct Recovery = 94% Analysis Date = 11/18/16 Pct Recovery = 94% Analysis Date = 11/18/16 Pct Recovery = 94% Analysis Date = 11/13/16 Pct Recovery = 94% Analysis Date = 11/13/16 Pct Recovery = 94% Analysis Date = 11/08/16 Pct Recovery = 93% Analysis Date = 11/08/16 Pct Recovery = 93% Analysis Date = 11/03/16 Pct Recovery = 93% Analysis Date = 11/03/16 Pct Recovery = 93% Analysis Date = 10/29/16 Pct Recovery = 93% Analysis Date = 10/29/16 Pct Recovery = 93% Analysis Date = 10/25/16 Pct Recovery = 93% Analysis Date = 10/25/16 Pct Recovery = 93% Analysis Date = 10/20/16 Pct Recovery = 93% Analysis Date = 10/20/16 Pct Recovery = 93% Analysis Date = 10/15/16 Pct Recovery = 93% Analysis Date = 10/15/16 Pct Recovery = 93% Analysis Date = 10/10/16 Pct Recovery = 93% Analysis Date = 10/10/16 Pct Recovery = 93% Analysis Date = 10/06/16 Pct Recovery = 93% Analysis Date = 10/06/16 Pct Recovery = 93% Analysis Date = 10/01/16 Pct Recovery = 92% Analysis Date = 10/01/16 Pct Recovery = 92% Analysis Date = 09/26/16 Pct Recovery = 92% Analysis Date = 09/26/16 Pct Recovery = 92% Analysis Date = 09/21/16 Pct Recovery = 92% Analysis Date = 09/21/16 Pct Recovery = 92% Analysis Date = 09/16/16 Pct Recovery = 92% Analysis Date = 09/16/16 Pct Recovery = 92% Analysis Date = 09/12/16 Pct Recovery = 92% Analysis Date = 09/12/16 Pct Recovery = 92% Analysis Date = 09/07/16 Pct Recovery = 92% Analysis Date = 09/07/16 Pct Recovery = 92% Analysis Date = 09/02/16 Pct Recovery = 92% Analysis Date = 09/02/16 Pct Recovery = 92% Analysis Date = 08/28/16 Pct Recovery = 92% Analysis Date = 08/28/16 Pct Recovery = 92% Analysis Date = 08/24/16 Pct Recovery = 91% Analysis Date = 08/24/16 Pct Recovery = 91% Analysis Date = 08/19/16 Pct Recovery = 91% Analysis Date = 08/19/16 Pct Recovery = 91% Analysis Date = 08/14/16 Pct Recovery = 91% Analysis Date = 08/14/16 Pct Recovery = 91% Analysis Date = 08/09/16 Pct Recovery = 91% Analysis Date = 08/09/16 Pct Recovery = 91% Analysis Date = 08/04/16 Pct Recovery = 91% Analysis Date = 08/04/16 Pct Recovery = 91% Analysis Date = 07/31/16 Pct Recovery = 91% Analysis Date = 07/31/16 Pct Recovery = 91% Analysis Date = 07/26/16 Pct Recovery = 91% Analysis Date = 07/26/16 Pct Recovery = 91% Analysis Date = 07/21/16 Pct Recovery = 91% Analysis Date = 07/21/16 Pct Recovery = 91% Analysis Date = 07/16/16 Pct Recovery = 91% Analysis Date = 07/16/16 Pct Recovery = 91% Analysis Date = 07/12/16 Pct Recovery = 90% Analysis Date = 07/12/16 Pct Recovery = 90% Analysis Date = 07/07/16 Pct Recovery = 90% Analysis Date = 07/07/16 Pct Recovery = 90% Analysis Date = 07/02/16 Pct Recovery = 90% Analysis Date = 07/02/16 Pct Recovery = 90% Analysis Date = 06/27/16 Pct Recovery = 90% Analysis Date = 06/27/16 Pct Recovery = 90% Analysis Date = 06/22/16 Pct Recovery = 90% Analysis Date = 06/22/16 Pct Recovery = 90% Analysis Date = 06/18/16 Pct Recovery = 90% Analysis Date = 06/18/16 Pct Recovery = 90% Analysis Date = 06/13/16 Pct Recovery = 90% Analysis Date = 06/13/16 Pct Recovery = 90% Analysis Date = 06/08/16 Pct Recovery = 90% Analysis Date = 06/08/16 Pct Recovery = 90% Analysis Date = 06/03/16 Pct Recovery = 90% Analysis Date = 06/03/16 Pct Recovery = 90% Analysis Date = 05/30/16 Pct Recovery = 90% Analysis Date = 05/30/16 Pct Recovery = 90% Analysis Date = 05/25/16 Pct Recovery = 90% Analysis Date = 05/25/16 Pct Recovery = 90% Analysis Date = 05/20/16 Pct Recovery = 90% Analysis Date = 05/20/16 Pct Recovery = 90% Analysis Date = 05/15/16 Pct Recovery = 90% Analysis Date = 05/15/16 Pct Recovery = 90% Analysis Date = 05/10/16 Pct Recovery = 89% Analysis Date = 05/10/16 Pct Recovery = 89% Analysis Date = 05/06/16 Pct Recovery = 89% Analysis Date = 05/06/16 Pct Recovery = 89% Analysis Date = 05/01/16 Pct Recovery = 89% Analysis Date = 05/01/16 Pct Recovery = 89% Analysis Date = 04/26/16 Pct Recovery = 89% Analysis Date = 04/26/16 Pct Recovery = 89% Analysis Date = 04/21/16 Pct Recovery = 89% Analysis Date = 04/21/16 Pct Recovery = 89% Analysis Date = 04/16/16 Pct Recovery = 89% Analysis Date = 04/16/16 Pct Recovery = 89% Analysis Date = 04/12/16 Pct Recovery = 89% Analysis Date = 04/12/16 Pct Recovery = 89% Analysis Date = 04/07/16 Pct Recovery = 89% Analysis Date = 04/07/16 Pct Recovery = 89% Analysis Date = 04/02/16 Pct Recovery = 89% Analysis Date = 04/02/16 Pct Recovery = 89% Analysis Date = 03/28/16 Pct Recovery = 89% Analysis Date = 03/28/16 Pct Recovery = 89% Analysis Date = 03/24/16 Pct Recovery = 89% Analysis Date = 03/24/16 Pct Recovery = 89% Analysis Date = 03/19/16 Pct Recovery = 89% Analysis Date = 03/19/16 Pct Recovery = 89% Analysis Date = 03/14/16 Pct Recovery = 89% Analysis Date = 03/14/16 Pct Recovery = 89% Analysis Date = 03/09/16 Pct Recovery = 89% Analysis Date = 03/09/16 Pct Recovery = 89% Analysis Date = 03/04/16 Pct Recovery = 89% Analysis Date = 03/04/16 Pct Recovery = 89% Analysis Date = 02/29/16 Pct Recovery = 89% Analysis Date = 02/29/16 Pct Recovery = 89% Analysis Date = 02/24/16 Pct Recovery = 89% Analysis Date = 02/24/16 Pct Recovery = 89% Analysis Date = 02/19/16 Pct Recovery = 89% Analysis Date = 02/19/16 Pct Recovery = 89% Analysis Date = 02/14/16 Pct Recovery = 90% Analysis Date = 02/14/16 Pct Recovery = 90% Analysis Date = 02/10/16 Pct Recovery = 90% Analysis Date = 02/10/16 Pct Recovery = 90% Analysis Date = 02/05/16 Pct Recovery = 90% Analysis Date = 02/05/16 Pct Recovery = 90% Analysis Date = 01/31/16 Pct Recovery = 90% Analysis Date = 01/31/16 Pct Recovery = 90% Analysis Date = 01/26/16 Pct Recovery = 90% Analysis Date = 01/26/16 Pct Recovery = 90% Analysis Date = 01/21/16 Pct Recovery = 90% Analysis Date = 01/21/16 Pct Recovery = 90% Analysis Date = 01/17/16 Pct Recovery = 90% Analysis Date = 01/17/16 Pct Recovery = 90% Analysis Date = 01/12/16 Pct Recovery = 90% Analysis Date = 01/12/16 Pct Recovery = 90% Analysis Date = 01/07/16 Pct Recovery = 90% Analysis Date = 01/07/16 Pct Recovery = 90% Analysis Date = 01/02/16 Pct Recovery = 90% Analysis Date = 01/02/16 Pct Recovery = 90% Analysis Date = 12/29/15 Pct Recovery = 90% Analysis Date = 12/29/15 Pct Recovery = 90% Analysis Date = 12/24/15 Pct Recovery = 90% Analysis Date = 12/24/15 Pct Recovery = 90% Analysis Date = 12/19/15 Pct Recovery = 90% Analysis Date = 12/19/15 Pct Recovery = 90% Analysis Date = 12/14/15 Pct Recovery = 91% Analysis Date = 12/14/15 Pct Recovery = 91% Analysis Date = 12/09/15 Pct Recovery = 91% Analysis Date = 12/09/15 Pct Recovery = 91% Analysis Date = 12/05/15 Pct Recovery = 91% Analysis Date = 12/05/15 Pct Recovery = 91% Analysis Date = 11/30/15 Pct Recovery = 91% Analysis Date = 11/30/15 Pct Recovery = 91% Analysis Date = 11/25/15 Pct Recovery = 91% Analysis Date = 11/25/15 Pct Recovery = 91% Analysis Date = 11/20/15 Pct Recovery = 91% Analysis Date = 11/20/15 Pct Recovery = 91% Analysis Date = 11/16/15 Pct Recovery = 91% Analysis Date = 11/16/15 Pct Recovery = 91% Analysis Date = 11/11/15 Pct Recovery = 91% Analysis Date = 11/11/15 Pct Recovery = 91% Analysis Date = 11/06/15 Pct Recovery = 91% Analysis Date = 11/06/15 Pct Recovery = 91% Analysis Date = 11/01/15 Pct Recovery = 92% Analysis Date = 11/01/15 Pct Recovery = 92% Analysis Date = 10/27/15 Pct Recovery = 92% Analysis Date = 10/27/15 Pct Recovery = 92% Analysis Date = 10/23/15 Pct Recovery = 92% Analysis Date = 10/23/15 Pct Recovery = 92% Analysis Date = 10/18/15 Pct Recovery = 92% Analysis Date = 10/18/15 Pct Recovery = 92% Analysis Date = 10/13/15 Pct Recovery = 92% Analysis Date = 10/13/15 Pct Recovery = 92% Analysis Date = 10/08/15 Pct Recovery = 92% Analysis Date = 10/08/15 Pct Recovery = 92% Analysis Date = 10/04/15 Pct Recovery = 92% Analysis Date = 10/04/15 Pct Recovery = 92% Analysis Date = 09/29/15 Pct Recovery = 93% Analysis Date = 09/29/15 Pct Recovery = 93% Analysis Date = 09/24/15 Pct Recovery = 93% Analysis Date = 09/24/15 Pct Recovery = 93% Analysis Date = 09/19/15 Pct Recovery = 93% Analysis Date = 09/19/15 Pct Recovery = 93% Analysis Date = 09/14/15 Pct Recovery = 93% Analysis Date = 09/14/15 Pct Recovery = 93% Analysis Date = 09/10/15 Pct Recovery = 93% Analysis Date = 09/10/15 Pct Recovery = 93% Analysis Date = 09/05/15 Pct Recovery = 93% Analysis Date = 09/05/15 Pct Recovery = 93% Analysis Date = 08/31/15 Pct Recovery = 93% Analysis Date = 08/31/15 Pct Recovery = 93% Analysis Date = 08/26/15 Pct Recovery = 93% Analysis Date = 08/26/15 Pct Recovery = 93% Analysis Date = 08/21/15 Pct Recovery = 94% Analysis Date = 08/21/15 Pct Recovery = 94% Analysis Date = 08/17/15 Pct Recovery = 94% Analysis Date = 08/17/15 Pct Recovery = 94% Analysis Date = 08/12/15 Pct Recovery = 94% Analysis Date = 08/12/15 Pct Recovery = 94% Analysis Date = 08/07/15 Pct Recovery = 94% Analysis Date = 08/07/15 Pct Recovery = 94% Analysis Date = 08/02/15 Pct Recovery = 94% Analysis Date = 08/02/15 Pct Recovery = 94% Analysis Date = 07/29/15 Pct Recovery = 94% Analysis Date = 07/29/15 Pct Recovery = 94% Analysis Date = 07/24/15 Pct Recovery = 94% Analysis Date = 07/24/15 Pct Recovery = 94% Analysis Date = 07/19/15 Pct Recovery = 94% Analysis Date = 07/19/15 Pct Recovery = 94% Analysis Date = 07/14/15 Pct Recovery = 94% Analysis Date = 07/14/15 Pct Recovery = 94% Analysis Date = 07/09/15 Pct Recovery = 94% Analysis Date = 07/09/15 Pct Recovery = 94% Analysis Date = 07/05/15 Pct Recovery = 94% Analysis Date = 07/05/15 Pct Recovery = 94% Analysis Date = 06/30/15 Pct Recovery = 94% Analysis Date = 06/30/15 Pct Recovery = 94% Analysis Date = 06/25/15 Pct Recovery = 95% Analysis Date = 06/25/15 Pct Recovery = 95% Analysis Date = 06/20/15 Pct Recovery = 95% Analysis Date = 06/20/15 Pct Recovery = 95% Analysis Date = 06/16/15 Pct Recovery = 95% Analysis Date = 06/16/15 Pct Recovery = 95% Analysis Date = 06/11/15 Pct Recovery = 95% Analysis Date = 06/11/15 Pct Recovery = 95% Analysis Date = 06/06/15 Pct Recovery = 95% Analysis Date = 06/06/15 Pct Recovery = 95% Analysis Date = 06/01/15 Pct Recovery = 95% Analysis Date = 06/01/15 Pct Recovery = 95% Analysis Date = 05/27/15 Pct Recovery = 95% Analysis Date = 05/27/15 Pct Recovery = 95% Analysis Date = 05/23/15 Pct Recovery = 95% Analysis Date = 05/23/15 Pct Recovery = 95% Analysis Date = 05/18/15 Pct Recovery = 95% Analysis Date = 05/18/15 Pct Recovery = 95% Analysis Date = 05/13/15 Pct Recovery = 95% Analysis Date = 05/13/15 Pct Recovery = 95% Analysis Date = 05/08/15 Pct Recovery = 95% Analysis Date = 05/08/15 Pct Recovery = 95% Analysis Date = 05/04/15 Pct Recovery = 95% Analysis Date = 05/04/15 Pct Recovery = 95% Analysis Date = 04/29/15 Pct Recovery = 95% Analysis Date = 04/29/15 Pct Recovery = 95% Analysis Date = 04/24/15 Pct Recovery = 95% Analysis Date = 04/24/15 Pct Recovery = 95% Analysis Date = 04/19/15 Pct Recovery = 95% Analysis Date = 04/19/15 Pct Recovery = 95% Analysis Date = 04/14/15 Pct Recovery = 95% Analysis Date = 04/14/15 Pct Recovery = 95% Analysis Date = 04/10/15 Pct Recovery = 95% Analysis Date = 04/10/15 Pct Recovery = 95% Analysis Date = 04/05/15 Pct Recovery = 95% Analysis Date = 04/05/15 Pct Recovery = 95% Analysis Date = 03/31/15 Pct Recovery = 95% Analysis Date = 03/31/15 Pct Recovery = 95% Analysis Date = 03/26/15 Pct Recovery = 95% Analysis Date = 03/26/15 Pct Recovery = 95% Analysis Date = 03/22/15 Pct Recovery = 96% Analysis Date = 03/22/15 Pct Recovery = 96% Analysis Date = 03/17/15 Pct Recovery = 96% Analysis Date = 03/17/15 Pct Recovery = 96% Analysis Date = 03/12/15 Pct Recovery = 96% Analysis Date = 03/12/15 Pct Recovery = 96% Analysis Date = 03/07/15 Pct Recovery = 96% Analysis Date = 03/07/15 Pct Recovery = 96% Analysis Date = 03/02/15 Pct Recovery = 96% Analysis Date = 03/02/15 Pct Recovery = 96% Analysis Date = 02/26/15 Pct Recovery = 96% Analysis Date = 02/26/15 Pct Recovery = 96% Analysis Date = 02/21/15 Pct Recovery = 96% Analysis Date = 02/21/15 Pct Recovery = 96% Analysis Date = 02/16/15 Pct Recovery = 96% Analysis Date = 02/16/15 Pct Recovery = 96% Analysis Date = 02/11/15 Pct Recovery = 96% Analysis Date = 02/11/15 Pct Recovery = 96% Analysis Date = 02/07/15 Pct Recovery = 96% Analysis Date = 02/07/15 Pct Recovery = 96% Analysis Date = 02/02/15 Pct Recovery = 96% Analysis Date = 02/02/15 Pct Recovery = 96% Analysis Date = 01/28/15 Pct Recovery = 96% Analysis Date = 01/28/15 Pct Recovery = 96% Analysis Date = 01/23/15 Pct Recovery = 96% Analysis Date = 01/23/15 Pct Recovery = 96% Analysis Date = 01/18/15 Pct Recovery = 96% Analysis Date = 01/18/15 Pct Recovery = 96% Analysis Date = 01/14/15 Pct Recovery = 96% Analysis Date = 01/14/15 Pct Recovery = 96% Analysis Date = 01/09/15 Pct Recovery = 96% Analysis Date = 01/09/15 Pct Recovery = 96% Analysis Date = 01/04/15 Pct Recovery = 96% Analysis Date = 01/04/15 Pct Recovery = 96% Analysis Date = 12/30/14 Pct Recovery = 96% Analysis Date = 12/30/14 Pct Recovery = 96% Analysis Date = 12/25/14 Pct Recovery = 97% Analysis Date = 12/25/14 Pct Recovery = 97% Analysis Date = 12/21/14 Pct Recovery = 97% Analysis Date = 12/21/14 Pct Recovery = 97% Analysis Date = 12/16/14 Pct Recovery = 97% Analysis Date = 12/16/14 Pct Recovery = 97% Analysis Date = 12/11/14 Pct Recovery = 97% Analysis Date = 12/11/14 Pct Recovery = 97% Analysis Date = 12/06/14 Pct Recovery = 97% Analysis Date = 12/06/14 Pct Recovery = 97% Analysis Date = 12/02/14 Pct Recovery = 97% Analysis Date = 12/02/14 Pct Recovery = 97% Analysis Date = 11/27/14 Pct Recovery = 97% Analysis Date = 11/27/14 Pct Recovery = 97% Analysis Date = 11/22/14 Pct Recovery = 97% Analysis Date = 11/22/14 Pct Recovery = 97% Analysis Date = 11/17/14 Pct Recovery = 97% Analysis Date = 11/17/14 Pct Recovery = 97% Analysis Date = 11/12/14 Pct Recovery = 97% Analysis Date = 11/12/14 Pct Recovery = 97% Analysis Date = 11/08/14 Pct Recovery = 98% Analysis Date = 11/08/14 Pct Recovery = 98% Analysis Date = 11/03/14 Pct Recovery = 98% Analysis Date = 11/03/14 Pct Recovery = 98% Analysis Date = 10/29/14 Pct Recovery = 98% Analysis Date = 10/29/14 Pct Recovery = 98% Analysis Date = 10/24/14 Pct Recovery = 98% Analysis Date = 10/24/14 Pct Recovery = 98% Analysis Date = 10/20/14 Pct Recovery = 98% Analysis Date = 10/20/14 Pct Recovery = 98% Analysis Date = 10/15/14 Pct Recovery = 98% Analysis Date = 10/15/14 Pct Recovery = 98% Analysis Date = 10/10/14 Pct Recovery = 98% Analysis Date = 10/10/14 Pct Recovery = 98% Analysis Date = 10/05/14 Pct Recovery = 98% Analysis Date = 10/05/14 Pct Recovery = 98% Analysis Date = 09/30/14 Pct Recovery = 98% Analysis Date = 09/30/14 Pct Recovery = 98% Analysis Date = 09/26/14 Pct Recovery = 99% Analysis Date = 09/26/14 Pct Recovery = 99% Analysis Date = 09/21/14 Pct Recovery = 99% Analysis Date = 09/21/14 Pct Recovery = 99% Analysis Date = 09/16/14 Pct Recovery = 99% Analysis Date = 09/16/14 Pct Recovery = 99% Analysis Date = 09/11/14 Pct Recovery = 99% Analysis Date = 09/11/14 Pct Recovery = 99% Analysis Date = 09/07/14 Pct Recovery = 99% Analysis Date = 09/07/14 Pct Recovery = 99% Analysis Date = 09/02/14 Pct Recovery = 99% Analysis Date = 09/02/14 Pct Recovery = 99% Analysis Date = 08/28/14 Pct Recovery = 99% Analysis Date = 08/28/14 Pct Recovery = 99% Analysis Date = 08/23/14 Pct Recovery = 99% Analysis Date = 08/23/14 Pct Recovery = 99% Analysis Date = 08/18/14 Pct Recovery = 99% Analysis Date = 08/18/14 Pct Recovery = 99% Analysis Date = 08/14/14 Pct Recovery = 99% Analysis Date = 08/14/14 Pct Recovery = 99% Analysis Date = 08/09/14 Pct Recovery = 100% Analysis Date = 08/09/14 Pct Recovery = 100% Analysis Date = 08/04/14 Pct Recovery = 100% Analysis Date = 08/04/14 Pct Recovery = 100% Analysis Date = 07/30/14 Pct Recovery = 100% Analysis Date = 07/30/14 Pct Recovery = 100% Analysis Date = 07/26/14 Pct Recovery = 100% Analysis Date = 07/26/14 Pct Recovery = 100% Analysis Date = 07/21/14 Pct Recovery = 100% Analysis Date = 07/21/14 Pct Recovery = 100% Analysis Date = 07/16/14 Pct Recovery = 100% Analysis Date = 07/16/14 Pct Recovery = 100% Analysis Date = 07/11/14 Pct Recovery = 100% Analysis Date = 07/11/14 Pct Recovery = 100% Analysis Date = 07/06/14 Pct Recovery = 100% Analysis Date = 07/06/14 Pct Recovery = 100% Analysis Date = 07/02/14 Pct Recovery = 100% Analysis Date = 07/02/14 Pct Recovery = 100% Analysis Date = 06/27/14 Pct Recovery = 101% Analysis Date = 06/27/14 Pct Recovery = 101% Analysis Date = 06/22/14 Pct Recovery = 101% Analysis Date = 06/22/14 Pct Recovery = 101% Analysis Date = 06/17/14 Pct Recovery = 101% Analysis Date = 06/17/14 Pct Recovery = 101% Analysis Date = 06/13/14 Pct Recovery = 101% Analysis Date = 06/13/14 Pct Recovery = 101% Analysis Date = 06/08/14 Pct Recovery = 101% Analysis Date = 06/08/14 Pct Recovery = 101% Analysis Date = 06/03/14 Pct Recovery = 101% Analysis Date = 06/03/14 Pct Recovery = 101% Analysis Date = 05/29/14 Pct Recovery = 101% Analysis Date = 05/29/14 Pct Recovery = 101% Analysis Date = 05/24/14 Pct Recovery = 101% Analysis Date = 05/24/14 Pct Recovery = 101% Analysis Date = 05/20/14 Pct Recovery = 102% Analysis Date = 05/20/14 Pct Recovery = 102% Analysis Date = 05/15/14 Pct Recovery = 102% Analysis Date = 05/15/14 Pct Recovery = 102% Analysis Date = 05/10/14 Pct Recovery = 102% Analysis Date = 05/10/14 Pct Recovery = 102% Analysis Date = 05/05/14 Pct Recovery = 102% Analysis Date = 05/05/14 Pct Recovery = 102% Analysis Date = 05/01/14 Pct Recovery = 102% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
2-BUTANONE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 48 94% 12% 94% 13%
Total 48 94% 12% 94% 13%

Sample Statistics
2-BUTANONE

Characteristic N % % Basis
Plotted 48 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 48 .  
False Negatives 0 0% 0 out of 48
Not Spiked 25 .  
False Positives 0 0% 0 out of 25

BQS OBSP Determination:
2-CHLOROTOLUENE
METHOD: 4440 , TESTIDCODE: 77275GCM66
Open Data Set

Analysis Date = 12/16/16 SpikeMix = NSI 041816AVOC: 40 µl & ChemService 5082900: 40 µl Pct Recovery = 95% Analysis Date = 08/04/16 SpikeMix = Crescent 03FF058: 40 µl & Supelco LC20141V: 40 µl Pct Recovery = 89% Analysis Date = 07/20/16 SpikeMix = Supelco LC20141V: 40 µl & Accu 216041125: 40 µl Pct Recovery = 100% Analysis Date = 04/09/15 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 81% Analysis Date = 08/19/14 SpikeMix = Spex Organics C1140417015: 20 µl & Accu 214031115: 20 µl Pct Recovery = 101% Analysis Date = 07/01/14 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 88% Analysis Date = 05/01/14 SpikeMix = Accu 214031115: 20 µl & NSI 032614: 20 µl Pct Recovery = 72% Analysis Date = 08/26/16 SpikeMix = NSI 041816AVOC: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 95% Analysis Date = 08/12/16 SpikeMix = ChemService 5082900: 25 µl & Phenova B20160319: 25 µl Pct Recovery = 100% Analysis Date = 06/30/16 SpikeMix = Crescent 03FF058: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 91% Analysis Date = 11/21/16 SpikeMix = Crescent 03FF058: 25 µl & Supelco LC20141V: 25 µl Pct Recovery = 87% Analysis Date = 09/08/16 SpikeMix = Supelco LC20141V: 25 µl & Accu 216041125: 25 µl Pct Recovery = 88% Analysis Date = 03/19/15 SpikeMix = Spex Organics C1140417015: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 147% Analysis Date = 12/17/14 SpikeMix = Supelco LC06438: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 129% Analysis Date = 11/14/14 SpikeMix = Crescent 03DD004: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 117% Analysis Date = 06/10/14 SpikeMix = Crescent 03DD004: 20 µl & NSI 032614: 20 µl Pct Recovery = 100% Analysis Date = 08/15/15 SpikeMix = Supelco LC13545: 25 µl & Crescent 04EE008: 25 µl Pct Recovery = 100% Analysis Date = 06/16/15 SpikeMix = ERA 0406-15-03: 25 µl & Supelco LC13545: 25 µl Pct Recovery = 87% Analysis Date = 11/29/16 SpikeMix = ChemService 5082900: 15 µl & Phenova B20160319: 15 µl Pct Recovery = 96% Analysis Date = 09/28/16 SpikeMix = Crescent 03FF058: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 91% Analysis Date = 06/30/16 SpikeMix = ChemService 5082900: 15 µl & Accu 216041125: 15 µl Pct Recovery = 99% Analysis Date = 06/10/16 SpikeMix = NSI 041816AVOC: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 101% Analysis Date = 10/13/16 SpikeMix = NSI 041816AVOC: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 85% Analysis Date = 05/27/16 SpikeMix = Phenova B20160319: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 98% Analysis Date = 04/26/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 89% Analysis Date = 02/05/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 100% Analysis Date = 11/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 83% Analysis Date = 10/16/15 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 93% Analysis Date = 05/09/15 SpikeMix = Spex Organics EN150428007: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 118% Analysis Date = 04/02/16 SpikeMix = Supelco LC13545: 15 µl & Accu 215041380: 15 µl Pct Recovery = 91% Analysis Date = 12/18/15 SpikeMix = Supelco LC13545: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 89% Analysis Date = 01/13/15 SpikeMix = Accu 214031115: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 86% Analysis Date = 09/09/14 SpikeMix = Accu 214031115: 10 µl & NSI 032614: 10 µl Pct Recovery = 91% Analysis Date = 07/23/14 SpikeMix = Spex Organics C1140417015: 10 µl & Accu 214031115: 10 µl Pct Recovery = 114% Analysis Date = 06/18/14 SpikeMix = Supelco LC06438: 10 µl & Accu 214031115: 10 µl Pct Recovery = 92% Analysis Date = 11/06/14 SpikeMix = Spex Organics C1140417015: 10 µl & Crescent 03DD004: 10 µl Pct Recovery = 141% Analysis Date = 10/04/14 SpikeMix = Crescent 03DD004: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 123% Analysis Date = 07/29/14 SpikeMix = Crescent 03DD004: 10 µl & NSI 032614: 10 µl Pct Recovery = 125% Analysis Date = 05/03/14 SpikeMix = Crescent 03DD004: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 144% Analysis Date = 02/18/16 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 104% Analysis Date = 11/12/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 92% Analysis Date = 09/03/15 SpikeMix = NSI 050515AVOC: 10 µl & Spex Organics EN150428007: 10 µl Pct Recovery = 90% Analysis Date = 05/21/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 115% Analysis Date = 05/13/16 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 107% Analysis Date = 03/17/16 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 88% Analysis Date = 12/10/15 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 94% Analysis Date = 06/27/15 SpikeMix = ERA 0406-15-03: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 97% Analysis Date = 05/09/15 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 97% Analysis Date = 12/15/16 Pct Recovery = 92% Analysis Date = 12/11/16 Pct Recovery = 92% Analysis Date = 12/11/16 Pct Recovery = 92% Analysis Date = 12/06/16 Pct Recovery = 93% Analysis Date = 12/06/16 Pct Recovery = 93% Analysis Date = 12/01/16 Pct Recovery = 93% Analysis Date = 12/01/16 Pct Recovery = 93% Analysis Date = 11/26/16 Pct Recovery = 93% Analysis Date = 11/26/16 Pct Recovery = 93% Analysis Date = 11/21/16 Pct Recovery = 93% Analysis Date = 11/21/16 Pct Recovery = 93% Analysis Date = 11/17/16 Pct Recovery = 93% Analysis Date = 11/17/16 Pct Recovery = 93% Analysis Date = 11/12/16 Pct Recovery = 93% Analysis Date = 11/12/16 Pct Recovery = 93% Analysis Date = 11/07/16 Pct Recovery = 93% Analysis Date = 11/07/16 Pct Recovery = 93% Analysis Date = 11/02/16 Pct Recovery = 93% Analysis Date = 11/02/16 Pct Recovery = 93% Analysis Date = 10/28/16 Pct Recovery = 93% Analysis Date = 10/28/16 Pct Recovery = 93% Analysis Date = 10/24/16 Pct Recovery = 93% Analysis Date = 10/24/16 Pct Recovery = 93% Analysis Date = 10/19/16 Pct Recovery = 93% Analysis Date = 10/19/16 Pct Recovery = 93% Analysis Date = 10/14/16 Pct Recovery = 93% Analysis Date = 10/14/16 Pct Recovery = 93% Analysis Date = 10/09/16 Pct Recovery = 93% Analysis Date = 10/09/16 Pct Recovery = 93% Analysis Date = 10/04/16 Pct Recovery = 93% Analysis Date = 10/04/16 Pct Recovery = 93% Analysis Date = 09/30/16 Pct Recovery = 93% Analysis Date = 09/30/16 Pct Recovery = 93% Analysis Date = 09/25/16 Pct Recovery = 93% Analysis Date = 09/25/16 Pct Recovery = 93% Analysis Date = 09/20/16 Pct Recovery = 93% Analysis Date = 09/20/16 Pct Recovery = 93% Analysis Date = 09/15/16 Pct Recovery = 93% Analysis Date = 09/15/16 Pct Recovery = 93% Analysis Date = 09/10/16 Pct Recovery = 94% Analysis Date = 09/10/16 Pct Recovery = 94% Analysis Date = 09/06/16 Pct Recovery = 94% Analysis Date = 09/06/16 Pct Recovery = 94% Analysis Date = 09/01/16 Pct Recovery = 94% Analysis Date = 09/01/16 Pct Recovery = 94% Analysis Date = 08/27/16 Pct Recovery = 94% Analysis Date = 08/27/16 Pct Recovery = 94% Analysis Date = 08/22/16 Pct Recovery = 94% Analysis Date = 08/22/16 Pct Recovery = 94% Analysis Date = 08/17/16 Pct Recovery = 94% Analysis Date = 08/17/16 Pct Recovery = 94% Analysis Date = 08/13/16 Pct Recovery = 94% Analysis Date = 08/13/16 Pct Recovery = 94% Analysis Date = 08/08/16 Pct Recovery = 94% Analysis Date = 08/08/16 Pct Recovery = 94% Analysis Date = 08/03/16 Pct Recovery = 94% Analysis Date = 08/03/16 Pct Recovery = 94% Analysis Date = 07/29/16 Pct Recovery = 94% Analysis Date = 07/29/16 Pct Recovery = 94% Analysis Date = 07/24/16 Pct Recovery = 94% Analysis Date = 07/24/16 Pct Recovery = 94% Analysis Date = 07/20/16 Pct Recovery = 94% Analysis Date = 07/20/16 Pct Recovery = 94% Analysis Date = 07/15/16 Pct Recovery = 94% Analysis Date = 07/15/16 Pct Recovery = 94% Analysis Date = 07/10/16 Pct Recovery = 94% Analysis Date = 07/10/16 Pct Recovery = 94% Analysis Date = 07/05/16 Pct Recovery = 94% Analysis Date = 07/05/16 Pct Recovery = 94% Analysis Date = 06/30/16 Pct Recovery = 94% Analysis Date = 06/30/16 Pct Recovery = 94% Analysis Date = 06/26/16 Pct Recovery = 94% Analysis Date = 06/26/16 Pct Recovery = 94% Analysis Date = 06/21/16 Pct Recovery = 94% Analysis Date = 06/21/16 Pct Recovery = 94% Analysis Date = 06/16/16 Pct Recovery = 94% Analysis Date = 06/16/16 Pct Recovery = 94% Analysis Date = 06/11/16 Pct Recovery = 94% Analysis Date = 06/11/16 Pct Recovery = 94% Analysis Date = 06/06/16 Pct Recovery = 94% Analysis Date = 06/06/16 Pct Recovery = 94% Analysis Date = 06/02/16 Pct Recovery = 94% Analysis Date = 06/02/16 Pct Recovery = 94% Analysis Date = 05/28/16 Pct Recovery = 94% Analysis Date = 05/28/16 Pct Recovery = 94% Analysis Date = 05/23/16 Pct Recovery = 94% Analysis Date = 05/23/16 Pct Recovery = 94% Analysis Date = 05/18/16 Pct Recovery = 94% Analysis Date = 05/18/16 Pct Recovery = 94% Analysis Date = 05/13/16 Pct Recovery = 94% Analysis Date = 05/13/16 Pct Recovery = 94% Analysis Date = 05/09/16 Pct Recovery = 94% Analysis Date = 05/09/16 Pct Recovery = 94% Analysis Date = 05/04/16 Pct Recovery = 94% Analysis Date = 05/04/16 Pct Recovery = 94% Analysis Date = 04/29/16 Pct Recovery = 94% Analysis Date = 04/29/16 Pct Recovery = 94% Analysis Date = 04/24/16 Pct Recovery = 94% Analysis Date = 04/24/16 Pct Recovery = 94% Analysis Date = 04/19/16 Pct Recovery = 94% Analysis Date = 04/19/16 Pct Recovery = 94% Analysis Date = 04/15/16 Pct Recovery = 94% Analysis Date = 04/15/16 Pct Recovery = 94% Analysis Date = 04/10/16 Pct Recovery = 94% Analysis Date = 04/10/16 Pct Recovery = 94% Analysis Date = 04/05/16 Pct Recovery = 94% Analysis Date = 04/05/16 Pct Recovery = 94% Analysis Date = 03/31/16 Pct Recovery = 94% Analysis Date = 03/31/16 Pct Recovery = 94% Analysis Date = 03/26/16 Pct Recovery = 94% Analysis Date = 03/26/16 Pct Recovery = 94% Analysis Date = 03/22/16 Pct Recovery = 94% Analysis Date = 03/22/16 Pct Recovery = 94% Analysis Date = 03/17/16 Pct Recovery = 94% Analysis Date = 03/17/16 Pct Recovery = 94% Analysis Date = 03/12/16 Pct Recovery = 94% Analysis Date = 03/12/16 Pct Recovery = 94% Analysis Date = 03/07/16 Pct Recovery = 94% Analysis Date = 03/07/16 Pct Recovery = 94% Analysis Date = 03/02/16 Pct Recovery = 94% Analysis Date = 03/02/16 Pct Recovery = 94% Analysis Date = 02/27/16 Pct Recovery = 94% Analysis Date = 02/27/16 Pct Recovery = 94% Analysis Date = 02/22/16 Pct Recovery = 94% Analysis Date = 02/22/16 Pct Recovery = 94% Analysis Date = 02/17/16 Pct Recovery = 94% Analysis Date = 02/17/16 Pct Recovery = 94% Analysis Date = 02/12/16 Pct Recovery = 94% Analysis Date = 02/12/16 Pct Recovery = 94% Analysis Date = 02/07/16 Pct Recovery = 94% Analysis Date = 02/07/16 Pct Recovery = 94% Analysis Date = 02/03/16 Pct Recovery = 94% Analysis Date = 02/03/16 Pct Recovery = 94% Analysis Date = 01/29/16 Pct Recovery = 94% Analysis Date = 01/29/16 Pct Recovery = 94% Analysis Date = 01/24/16 Pct Recovery = 94% Analysis Date = 01/24/16 Pct Recovery = 94% Analysis Date = 01/19/16 Pct Recovery = 94% Analysis Date = 01/19/16 Pct Recovery = 94% Analysis Date = 01/14/16 Pct Recovery = 94% Analysis Date = 01/14/16 Pct Recovery = 94% Analysis Date = 01/10/16 Pct Recovery = 94% Analysis Date = 01/10/16 Pct Recovery = 94% Analysis Date = 01/05/16 Pct Recovery = 94% Analysis Date = 01/05/16 Pct Recovery = 94% Analysis Date = 12/31/15 Pct Recovery = 94% Analysis Date = 12/31/15 Pct Recovery = 94% Analysis Date = 12/26/15 Pct Recovery = 94% Analysis Date = 12/26/15 Pct Recovery = 94% Analysis Date = 12/21/15 Pct Recovery = 94% Analysis Date = 12/21/15 Pct Recovery = 94% Analysis Date = 12/17/15 Pct Recovery = 94% Analysis Date = 12/17/15 Pct Recovery = 94% Analysis Date = 12/12/15 Pct Recovery = 94% Analysis Date = 12/12/15 Pct Recovery = 94% Analysis Date = 12/07/15 Pct Recovery = 94% Analysis Date = 12/07/15 Pct Recovery = 94% Analysis Date = 12/02/15 Pct Recovery = 94% Analysis Date = 12/02/15 Pct Recovery = 94% Analysis Date = 11/27/15 Pct Recovery = 95% Analysis Date = 11/27/15 Pct Recovery = 95% Analysis Date = 11/23/15 Pct Recovery = 95% Analysis Date = 11/23/15 Pct Recovery = 95% Analysis Date = 11/18/15 Pct Recovery = 95% Analysis Date = 11/18/15 Pct Recovery = 95% Analysis Date = 11/13/15 Pct Recovery = 95% Analysis Date = 11/13/15 Pct Recovery = 95% Analysis Date = 11/08/15 Pct Recovery = 95% Analysis Date = 11/08/15 Pct Recovery = 95% Analysis Date = 11/03/15 Pct Recovery = 95% Analysis Date = 11/03/15 Pct Recovery = 95% Analysis Date = 10/30/15 Pct Recovery = 96% Analysis Date = 10/30/15 Pct Recovery = 96% Analysis Date = 10/25/15 Pct Recovery = 96% Analysis Date = 10/25/15 Pct Recovery = 96% Analysis Date = 10/20/15 Pct Recovery = 96% Analysis Date = 10/20/15 Pct Recovery = 96% Analysis Date = 10/15/15 Pct Recovery = 96% Analysis Date = 10/15/15 Pct Recovery = 96% Analysis Date = 10/10/15 Pct Recovery = 96% Analysis Date = 10/10/15 Pct Recovery = 96% Analysis Date = 10/06/15 Pct Recovery = 97% Analysis Date = 10/06/15 Pct Recovery = 97% Analysis Date = 10/01/15 Pct Recovery = 97% Analysis Date = 10/01/15 Pct Recovery = 97% Analysis Date = 09/26/15 Pct Recovery = 97% Analysis Date = 09/26/15 Pct Recovery = 97% Analysis Date = 09/21/15 Pct Recovery = 97% Analysis Date = 09/21/15 Pct Recovery = 97% Analysis Date = 09/16/15 Pct Recovery = 98% Analysis Date = 09/16/15 Pct Recovery = 98% Analysis Date = 09/12/15 Pct Recovery = 98% Analysis Date = 09/12/15 Pct Recovery = 98% Analysis Date = 09/07/15 Pct Recovery = 98% Analysis Date = 09/07/15 Pct Recovery = 98% Analysis Date = 09/02/15 Pct Recovery = 98% Analysis Date = 09/02/15 Pct Recovery = 98% Analysis Date = 08/28/15 Pct Recovery = 99% Analysis Date = 08/28/15 Pct Recovery = 99% Analysis Date = 08/23/15 Pct Recovery = 99% Analysis Date = 08/23/15 Pct Recovery = 99% Analysis Date = 08/19/15 Pct Recovery = 99% Analysis Date = 08/19/15 Pct Recovery = 99% Analysis Date = 08/14/15 Pct Recovery = 99% Analysis Date = 08/14/15 Pct Recovery = 99% Analysis Date = 08/09/15 Pct Recovery = 99% Analysis Date = 08/09/15 Pct Recovery = 99% Analysis Date = 08/04/15 Pct Recovery = 100% Analysis Date = 08/04/15 Pct Recovery = 100% Analysis Date = 07/30/15 Pct Recovery = 100% Analysis Date = 07/30/15 Pct Recovery = 100% Analysis Date = 07/26/15 Pct Recovery = 100% Analysis Date = 07/26/15 Pct Recovery = 100% Analysis Date = 07/21/15 Pct Recovery = 100% Analysis Date = 07/21/15 Pct Recovery = 100% Analysis Date = 07/16/15 Pct Recovery = 101% Analysis Date = 07/16/15 Pct Recovery = 101% Analysis Date = 07/11/15 Pct Recovery = 101% Analysis Date = 07/11/15 Pct Recovery = 101% Analysis Date = 07/06/15 Pct Recovery = 101% Analysis Date = 07/06/15 Pct Recovery = 101% Analysis Date = 07/02/15 Pct Recovery = 101% Analysis Date = 07/02/15 Pct Recovery = 101% Analysis Date = 06/27/15 Pct Recovery = 102% Analysis Date = 06/27/15 Pct Recovery = 102% Analysis Date = 06/22/15 Pct Recovery = 102% Analysis Date = 06/22/15 Pct Recovery = 102% Analysis Date = 06/17/15 Pct Recovery = 102% Analysis Date = 06/17/15 Pct Recovery = 102% Analysis Date = 06/12/15 Pct Recovery = 102% Analysis Date = 06/12/15 Pct Recovery = 102% Analysis Date = 06/08/15 Pct Recovery = 103% Analysis Date = 06/08/15 Pct Recovery = 103% Analysis Date = 06/03/15 Pct Recovery = 103% Analysis Date = 06/03/15 Pct Recovery = 103% Analysis Date = 05/29/15 Pct Recovery = 103% Analysis Date = 05/29/15 Pct Recovery = 103% Analysis Date = 05/24/15 Pct Recovery = 104% Analysis Date = 05/24/15 Pct Recovery = 104% Analysis Date = 05/19/15 Pct Recovery = 104% Analysis Date = 05/19/15 Pct Recovery = 104% Analysis Date = 05/15/15 Pct Recovery = 104% Analysis Date = 05/15/15 Pct Recovery = 104% Analysis Date = 05/10/15 Pct Recovery = 104% Analysis Date = 05/10/15 Pct Recovery = 104% Analysis Date = 05/05/15 Pct Recovery = 105% Analysis Date = 05/05/15 Pct Recovery = 105% Analysis Date = 04/30/15 Pct Recovery = 105% Analysis Date = 04/30/15 Pct Recovery = 105% Analysis Date = 04/25/15 Pct Recovery = 105% Analysis Date = 04/25/15 Pct Recovery = 105% Analysis Date = 04/21/15 Pct Recovery = 105% Analysis Date = 04/21/15 Pct Recovery = 105% Analysis Date = 04/16/15 Pct Recovery = 106% Analysis Date = 04/16/15 Pct Recovery = 106% Analysis Date = 04/11/15 Pct Recovery = 106% Analysis Date = 04/11/15 Pct Recovery = 106% Analysis Date = 04/06/15 Pct Recovery = 106% Analysis Date = 04/06/15 Pct Recovery = 106% Analysis Date = 04/01/15 Pct Recovery = 106% Analysis Date = 04/01/15 Pct Recovery = 106% Analysis Date = 03/28/15 Pct Recovery = 107% Analysis Date = 03/28/15 Pct Recovery = 107% Analysis Date = 03/23/15 Pct Recovery = 107% Analysis Date = 03/23/15 Pct Recovery = 107% Analysis Date = 03/18/15 Pct Recovery = 107% Analysis Date = 03/18/15 Pct Recovery = 107% Analysis Date = 03/13/15 Pct Recovery = 107% Analysis Date = 03/13/15 Pct Recovery = 107% Analysis Date = 03/08/15 Pct Recovery = 107% Analysis Date = 03/08/15 Pct Recovery = 107% Analysis Date = 03/04/15 Pct Recovery = 107% Analysis Date = 03/04/15 Pct Recovery = 107% Analysis Date = 02/27/15 Pct Recovery = 107% Analysis Date = 02/27/15 Pct Recovery = 107% Analysis Date = 02/22/15 Pct Recovery = 107% Analysis Date = 02/22/15 Pct Recovery = 107% Analysis Date = 02/17/15 Pct Recovery = 107% Analysis Date = 02/17/15 Pct Recovery = 107% Analysis Date = 02/12/15 Pct Recovery = 107% Analysis Date = 02/12/15 Pct Recovery = 107% Analysis Date = 02/08/15 Pct Recovery = 107% Analysis Date = 02/08/15 Pct Recovery = 107% Analysis Date = 02/03/15 Pct Recovery = 108% Analysis Date = 02/03/15 Pct Recovery = 108% Analysis Date = 01/29/15 Pct Recovery = 108% Analysis Date = 01/29/15 Pct Recovery = 108% Analysis Date = 01/24/15 Pct Recovery = 108% Analysis Date = 01/24/15 Pct Recovery = 108% Analysis Date = 01/19/15 Pct Recovery = 108% Analysis Date = 01/19/15 Pct Recovery = 108% Analysis Date = 01/15/15 Pct Recovery = 108% Analysis Date = 01/15/15 Pct Recovery = 108% Analysis Date = 01/10/15 Pct Recovery = 108% Analysis Date = 01/10/15 Pct Recovery = 108% Analysis Date = 01/05/15 Pct Recovery = 108% Analysis Date = 01/05/15 Pct Recovery = 108% Analysis Date = 12/31/14 Pct Recovery = 108% Analysis Date = 12/31/14 Pct Recovery = 108% Analysis Date = 12/26/14 Pct Recovery = 108% Analysis Date = 12/26/14 Pct Recovery = 108% Analysis Date = 12/22/14 Pct Recovery = 108% Analysis Date = 12/22/14 Pct Recovery = 108% Analysis Date = 12/17/14 Pct Recovery = 108% Analysis Date = 12/17/14 Pct Recovery = 108% Analysis Date = 12/12/14 Pct Recovery = 108% Analysis Date = 12/12/14 Pct Recovery = 108% Analysis Date = 12/07/14 Pct Recovery = 108% Analysis Date = 12/07/14 Pct Recovery = 108% Analysis Date = 12/02/14 Pct Recovery = 108% Analysis Date = 12/02/14 Pct Recovery = 108% Analysis Date = 11/28/14 Pct Recovery = 108% Analysis Date = 11/28/14 Pct Recovery = 108% Analysis Date = 11/23/14 Pct Recovery = 108% Analysis Date = 11/23/14 Pct Recovery = 108% Analysis Date = 11/18/14 Pct Recovery = 108% Analysis Date = 11/18/14 Pct Recovery = 108% Analysis Date = 11/13/14 Pct Recovery = 108% Analysis Date = 11/13/14 Pct Recovery = 108% Analysis Date = 11/08/14 Pct Recovery = 108% Analysis Date = 11/08/14 Pct Recovery = 108% Analysis Date = 11/04/14 Pct Recovery = 108% Analysis Date = 11/04/14 Pct Recovery = 108% Analysis Date = 10/30/14 Pct Recovery = 108% Analysis Date = 10/30/14 Pct Recovery = 108% Analysis Date = 10/25/14 Pct Recovery = 108% Analysis Date = 10/25/14 Pct Recovery = 108% Analysis Date = 10/20/14 Pct Recovery = 108% Analysis Date = 10/20/14 Pct Recovery = 108% Analysis Date = 10/15/14 Pct Recovery = 108% Analysis Date = 10/15/14 Pct Recovery = 108% Analysis Date = 10/11/14 Pct Recovery = 108% Analysis Date = 10/11/14 Pct Recovery = 108% Analysis Date = 10/06/14 Pct Recovery = 108% Analysis Date = 10/06/14 Pct Recovery = 108% Analysis Date = 10/01/14 Pct Recovery = 108% Analysis Date = 10/01/14 Pct Recovery = 108% Analysis Date = 09/26/14 Pct Recovery = 108% Analysis Date = 09/26/14 Pct Recovery = 108% Analysis Date = 09/21/14 Pct Recovery = 108% Analysis Date = 09/21/14 Pct Recovery = 108% Analysis Date = 09/17/14 Pct Recovery = 108% Analysis Date = 09/17/14 Pct Recovery = 108% Analysis Date = 09/12/14 Pct Recovery = 108% Analysis Date = 09/12/14 Pct Recovery = 108% Analysis Date = 09/07/14 Pct Recovery = 108% Analysis Date = 09/07/14 Pct Recovery = 108% Analysis Date = 09/02/14 Pct Recovery = 108% Analysis Date = 09/02/14 Pct Recovery = 108% Analysis Date = 08/28/14 Pct Recovery = 108% Analysis Date = 08/28/14 Pct Recovery = 108% Analysis Date = 08/24/14 Pct Recovery = 108% Analysis Date = 08/24/14 Pct Recovery = 108% Analysis Date = 08/19/14 Pct Recovery = 108% Analysis Date = 08/19/14 Pct Recovery = 108% Analysis Date = 08/14/14 Pct Recovery = 108% Analysis Date = 08/14/14 Pct Recovery = 108% Analysis Date = 08/09/14 Pct Recovery = 108% Analysis Date = 08/09/14 Pct Recovery = 108% Analysis Date = 08/04/14 Pct Recovery = 108% Analysis Date = 08/04/14 Pct Recovery = 108% Analysis Date = 07/31/14 Pct Recovery = 108% Analysis Date = 07/31/14 Pct Recovery = 108% Analysis Date = 07/26/14 Pct Recovery = 108% Analysis Date = 07/26/14 Pct Recovery = 108% Analysis Date = 07/21/14 Pct Recovery = 108% Analysis Date = 07/21/14 Pct Recovery = 108% Analysis Date = 07/16/14 Pct Recovery = 108% Analysis Date = 07/16/14 Pct Recovery = 108% Analysis Date = 07/11/14 Pct Recovery = 108% Analysis Date = 07/11/14 Pct Recovery = 108% Analysis Date = 07/07/14 Pct Recovery = 108% Analysis Date = 07/07/14 Pct Recovery = 108% Analysis Date = 07/02/14 Pct Recovery = 108% Analysis Date = 07/02/14 Pct Recovery = 108% Analysis Date = 06/27/14 Pct Recovery = 107% Analysis Date = 06/27/14 Pct Recovery = 107% Analysis Date = 06/22/14 Pct Recovery = 107% Analysis Date = 06/22/14 Pct Recovery = 107% Analysis Date = 06/17/14 Pct Recovery = 107% Analysis Date = 06/17/14 Pct Recovery = 107% Analysis Date = 06/13/14 Pct Recovery = 107% Analysis Date = 06/13/14 Pct Recovery = 107% Analysis Date = 06/08/14 Pct Recovery = 107% Analysis Date = 06/08/14 Pct Recovery = 107% Analysis Date = 06/03/14 Pct Recovery = 107% Analysis Date = 06/03/14 Pct Recovery = 107% Analysis Date = 05/29/14 Pct Recovery = 107% Analysis Date = 05/29/14 Pct Recovery = 107% Analysis Date = 05/24/14 Pct Recovery = 107% Analysis Date = 05/24/14 Pct Recovery = 107% Analysis Date = 05/20/14 Pct Recovery = 107% Analysis Date = 05/20/14 Pct Recovery = 107% Analysis Date = 05/15/14 Pct Recovery = 107% Analysis Date = 05/15/14 Pct Recovery = 107% Analysis Date = 05/10/14 Pct Recovery = 107% Analysis Date = 05/10/14 Pct Recovery = 107% Analysis Date = 05/05/14 Pct Recovery = 107% Analysis Date = 05/05/14 Pct Recovery = 107% Analysis Date = 05/01/14 Pct Recovery = 107% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
2-CHLOROTOLUENE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 48 100% 16% 96% 10%
Total 48 100% 16% 96% 10%

Sample Statistics
2-CHLOROTOLUENE

Characteristic N % % Basis
Plotted 48 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 48 .  
False Negatives 0 0% 0 out of 48
Not Spiked 25 .  
False Positives 0 0% 0 out of 25

BQS OBSP Determination:
2-HEXANONE
METHOD: 4440 , TESTIDCODE: 77103GCM66
Open Data Set

Analysis Date = 12/12/16 SpikeMix = Accu 216041125: 40 µl & Crescent 03FF058: 40 µl Pct Recovery = 114% Analysis Date = 08/04/16 SpikeMix = Crescent 03FF058: 40 µl & Supelco LC20141V: 40 µl Pct Recovery = 88% Analysis Date = 11/21/16 SpikeMix = Crescent 03FF058: 25 µl & Supelco LC20141V: 25 µl Pct Recovery = 97% Analysis Date = 06/30/16 SpikeMix = Crescent 03FF058: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 89% Analysis Date = 06/21/16 SpikeMix = Phenova B20160319: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 105% Analysis Date = 05/24/16 SpikeMix = Accu 216041125: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 106% Analysis Date = 08/15/15 SpikeMix = Supelco LC13545: 25 µl & Crescent 04EE008: 25 µl Pct Recovery = 101% Analysis Date = 06/16/15 SpikeMix = ERA 0406-15-03: 25 µl & Supelco LC13545: 25 µl Pct Recovery = 96% Analysis Date = 09/28/16 SpikeMix = Crescent 03FF058: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 97% Analysis Date = 09/08/16 SpikeMix = Phenova B20160319: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 77% Analysis Date = 08/20/16 SpikeMix = Accu 216041125: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 99% Analysis Date = 04/26/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 113% Analysis Date = 04/02/16 SpikeMix = Supelco LC13545: 15 µl & Accu 215041380: 15 µl Pct Recovery = 89% Analysis Date = 02/05/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 87% Analysis Date = 12/18/15 SpikeMix = Supelco LC13545: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 96% Analysis Date = 11/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 107% Analysis Date = 10/16/15 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 100% Analysis Date = 05/09/15 SpikeMix = Spex Organics EN150428007: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 91% Analysis Date = 05/13/16 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 100% Analysis Date = 03/17/16 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 93% Analysis Date = 02/18/16 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 97% Analysis Date = 12/10/15 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 103% Analysis Date = 11/12/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 87% Analysis Date = 09/03/15 SpikeMix = NSI 050515AVOC: 10 µl & Spex Organics EN150428007: 10 µl Pct Recovery = 80% Analysis Date = 06/27/15 SpikeMix = ERA 0406-15-03: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 93% Analysis Date = 05/21/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 103% Analysis Date = 05/09/15 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 93% Analysis Date = 09/21/14 SpikeMix = Supelco LC06438: 20 µl Pct Recovery = 121% Analysis Date = 08/19/14 SpikeMix = Spex Organics C1140417015: 20 µl & Accu 214031115: 20 µl Pct Recovery = 106% Analysis Date = 08/16/14 SpikeMix = ERA 0227-14-06.1A: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 99% Analysis Date = 06/10/14 SpikeMix = NSI 032614: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 91% Analysis Date = 09/09/14 SpikeMix = NSI 032614: 10 µl & Spex Organics C1140417015: 10 µl Pct Recovery = 125% Analysis Date = 07/23/14 SpikeMix = Spex Organics C1140417015: 10 µl & Accu 214031115: 10 µl Pct Recovery = 108% Analysis Date = 07/11/14 SpikeMix = Spex Organics C1140417015: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 113% Analysis Date = 06/18/14 SpikeMix = Supelco LC06438: 10 µl & Accu 214031115: 10 µl Pct Recovery = 109% Analysis Date = 05/30/14 SpikeMix = NSI 032614: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 122% Analysis Date = 05/03/14 SpikeMix = Crescent 03DD004: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 104% Analysis Date = 03/19/15 SpikeMix = Spex Organics C1140417015: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 106% Analysis Date = 03/06/15 SpikeMix = ERA 0227-14-06.1A: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 87% Analysis Date = 12/17/14 SpikeMix = Supelco LC06438: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 106% Analysis Date = 11/22/14 SpikeMix = NSI 032614: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 81% Analysis Date = 11/06/14 SpikeMix = Spex Organics C1140417015: 10 µl & Crescent 03DD004: 10 µl Pct Recovery = 113% Analysis Date = 10/21/14 SpikeMix = ERA 0227-14-06.1A: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 87% Analysis Date = 12/12/16 Pct Recovery = 99% Analysis Date = 12/07/16 Pct Recovery = 99% Analysis Date = 12/07/16 Pct Recovery = 99% Analysis Date = 12/02/16 Pct Recovery = 99% Analysis Date = 12/02/16 Pct Recovery = 99% Analysis Date = 11/27/16 Pct Recovery = 99% Analysis Date = 11/27/16 Pct Recovery = 99% Analysis Date = 11/22/16 Pct Recovery = 99% Analysis Date = 11/22/16 Pct Recovery = 99% Analysis Date = 11/18/16 Pct Recovery = 98% Analysis Date = 11/18/16 Pct Recovery = 98% Analysis Date = 11/13/16 Pct Recovery = 98% Analysis Date = 11/13/16 Pct Recovery = 98% Analysis Date = 11/08/16 Pct Recovery = 98% Analysis Date = 11/08/16 Pct Recovery = 98% Analysis Date = 11/03/16 Pct Recovery = 98% Analysis Date = 11/03/16 Pct Recovery = 98% Analysis Date = 10/30/16 Pct Recovery = 98% Analysis Date = 10/30/16 Pct Recovery = 98% Analysis Date = 10/25/16 Pct Recovery = 98% Analysis Date = 10/25/16 Pct Recovery = 98% Analysis Date = 10/20/16 Pct Recovery = 98% Analysis Date = 10/20/16 Pct Recovery = 98% Analysis Date = 10/15/16 Pct Recovery = 98% Analysis Date = 10/15/16 Pct Recovery = 98% Analysis Date = 10/10/16 Pct Recovery = 98% Analysis Date = 10/10/16 Pct Recovery = 98% Analysis Date = 10/06/16 Pct Recovery = 98% Analysis Date = 10/06/16 Pct Recovery = 98% Analysis Date = 10/01/16 Pct Recovery = 98% Analysis Date = 10/01/16 Pct Recovery = 98% Analysis Date = 09/26/16 Pct Recovery = 98% Analysis Date = 09/26/16 Pct Recovery = 98% Analysis Date = 09/21/16 Pct Recovery = 98% Analysis Date = 09/21/16 Pct Recovery = 98% Analysis Date = 09/17/16 Pct Recovery = 98% Analysis Date = 09/17/16 Pct Recovery = 98% Analysis Date = 09/12/16 Pct Recovery = 98% Analysis Date = 09/12/16 Pct Recovery = 98% Analysis Date = 09/07/16 Pct Recovery = 98% Analysis Date = 09/07/16 Pct Recovery = 98% Analysis Date = 09/02/16 Pct Recovery = 98% Analysis Date = 09/02/16 Pct Recovery = 98% Analysis Date = 08/29/16 Pct Recovery = 98% Analysis Date = 08/29/16 Pct Recovery = 98% Analysis Date = 08/24/16 Pct Recovery = 98% Analysis Date = 08/24/16 Pct Recovery = 98% Analysis Date = 08/19/16 Pct Recovery = 98% Analysis Date = 08/19/16 Pct Recovery = 98% Analysis Date = 08/14/16 Pct Recovery = 98% Analysis Date = 08/14/16 Pct Recovery = 98% Analysis Date = 08/09/16 Pct Recovery = 98% Analysis Date = 08/09/16 Pct Recovery = 98% Analysis Date = 08/05/16 Pct Recovery = 97% Analysis Date = 08/05/16 Pct Recovery = 97% Analysis Date = 07/31/16 Pct Recovery = 97% Analysis Date = 07/31/16 Pct Recovery = 97% Analysis Date = 07/26/16 Pct Recovery = 97% Analysis Date = 07/26/16 Pct Recovery = 97% Analysis Date = 07/21/16 Pct Recovery = 97% Analysis Date = 07/21/16 Pct Recovery = 97% Analysis Date = 07/17/16 Pct Recovery = 97% Analysis Date = 07/17/16 Pct Recovery = 97% Analysis Date = 07/12/16 Pct Recovery = 97% Analysis Date = 07/12/16 Pct Recovery = 97% Analysis Date = 07/07/16 Pct Recovery = 97% Analysis Date = 07/07/16 Pct Recovery = 97% Analysis Date = 07/02/16 Pct Recovery = 97% Analysis Date = 07/02/16 Pct Recovery = 97% Analysis Date = 06/28/16 Pct Recovery = 97% Analysis Date = 06/28/16 Pct Recovery = 97% Analysis Date = 06/23/16 Pct Recovery = 97% Analysis Date = 06/23/16 Pct Recovery = 97% Analysis Date = 06/18/16 Pct Recovery = 97% Analysis Date = 06/18/16 Pct Recovery = 97% Analysis Date = 06/13/16 Pct Recovery = 97% Analysis Date = 06/13/16 Pct Recovery = 97% Analysis Date = 06/08/16 Pct Recovery = 97% Analysis Date = 06/08/16 Pct Recovery = 97% Analysis Date = 06/04/16 Pct Recovery = 97% Analysis Date = 06/04/16 Pct Recovery = 97% Analysis Date = 05/30/16 Pct Recovery = 97% Analysis Date = 05/30/16 Pct Recovery = 97% Analysis Date = 05/25/16 Pct Recovery = 97% Analysis Date = 05/25/16 Pct Recovery = 97% Analysis Date = 05/20/16 Pct Recovery = 97% Analysis Date = 05/20/16 Pct Recovery = 97% Analysis Date = 05/16/16 Pct Recovery = 97% Analysis Date = 05/16/16 Pct Recovery = 97% Analysis Date = 05/11/16 Pct Recovery = 97% Analysis Date = 05/11/16 Pct Recovery = 97% Analysis Date = 05/06/16 Pct Recovery = 97% Analysis Date = 05/06/16 Pct Recovery = 97% Analysis Date = 05/01/16 Pct Recovery = 96% Analysis Date = 05/01/16 Pct Recovery = 96% Analysis Date = 04/27/16 Pct Recovery = 96% Analysis Date = 04/27/16 Pct Recovery = 96% Analysis Date = 04/22/16 Pct Recovery = 96% Analysis Date = 04/22/16 Pct Recovery = 96% Analysis Date = 04/17/16 Pct Recovery = 96% Analysis Date = 04/17/16 Pct Recovery = 96% Analysis Date = 04/12/16 Pct Recovery = 96% Analysis Date = 04/12/16 Pct Recovery = 96% Analysis Date = 04/07/16 Pct Recovery = 96% Analysis Date = 04/07/16 Pct Recovery = 96% Analysis Date = 04/03/16 Pct Recovery = 96% Analysis Date = 04/03/16 Pct Recovery = 96% Analysis Date = 03/29/16 Pct Recovery = 96% Analysis Date = 03/29/16 Pct Recovery = 96% Analysis Date = 03/24/16 Pct Recovery = 96% Analysis Date = 03/24/16 Pct Recovery = 96% Analysis Date = 03/19/16 Pct Recovery = 96% Analysis Date = 03/19/16 Pct Recovery = 96% Analysis Date = 03/15/16 Pct Recovery = 96% Analysis Date = 03/15/16 Pct Recovery = 96% Analysis Date = 03/10/16 Pct Recovery = 96% Analysis Date = 03/10/16 Pct Recovery = 96% Analysis Date = 03/05/16 Pct Recovery = 96% Analysis Date = 03/05/16 Pct Recovery = 96% Analysis Date = 02/29/16 Pct Recovery = 96% Analysis Date = 02/29/16 Pct Recovery = 96% Analysis Date = 02/25/16 Pct Recovery = 96% Analysis Date = 02/25/16 Pct Recovery = 96% Analysis Date = 02/20/16 Pct Recovery = 96% Analysis Date = 02/20/16 Pct Recovery = 96% Analysis Date = 02/15/16 Pct Recovery = 96% Analysis Date = 02/15/16 Pct Recovery = 96% Analysis Date = 02/10/16 Pct Recovery = 96% Analysis Date = 02/10/16 Pct Recovery = 96% Analysis Date = 02/05/16 Pct Recovery = 96% Analysis Date = 02/05/16 Pct Recovery = 96% Analysis Date = 02/01/16 Pct Recovery = 96% Analysis Date = 02/01/16 Pct Recovery = 96% Analysis Date = 01/27/16 Pct Recovery = 96% Analysis Date = 01/27/16 Pct Recovery = 96% Analysis Date = 01/22/16 Pct Recovery = 96% Analysis Date = 01/22/16 Pct Recovery = 96% Analysis Date = 01/17/16 Pct Recovery = 96% Analysis Date = 01/17/16 Pct Recovery = 96% Analysis Date = 01/13/16 Pct Recovery = 96% Analysis Date = 01/13/16 Pct Recovery = 96% Analysis Date = 01/08/16 Pct Recovery = 96% Analysis Date = 01/08/16 Pct Recovery = 96% Analysis Date = 01/03/16 Pct Recovery = 96% Analysis Date = 01/03/16 Pct Recovery = 96% Analysis Date = 12/29/15 Pct Recovery = 96% Analysis Date = 12/29/15 Pct Recovery = 96% Analysis Date = 12/25/15 Pct Recovery = 96% Analysis Date = 12/25/15 Pct Recovery = 96% Analysis Date = 12/20/15 Pct Recovery = 96% Analysis Date = 12/20/15 Pct Recovery = 96% Analysis Date = 12/15/15 Pct Recovery = 96% Analysis Date = 12/15/15 Pct Recovery = 96% Analysis Date = 12/10/15 Pct Recovery = 96% Analysis Date = 12/10/15 Pct Recovery = 96% Analysis Date = 12/05/15 Pct Recovery = 96% Analysis Date = 12/05/15 Pct Recovery = 96% Analysis Date = 12/01/15 Pct Recovery = 96% Analysis Date = 12/01/15 Pct Recovery = 96% Analysis Date = 11/26/15 Pct Recovery = 96% Analysis Date = 11/26/15 Pct Recovery = 96% Analysis Date = 11/21/15 Pct Recovery = 96% Analysis Date = 11/21/15 Pct Recovery = 96% Analysis Date = 11/16/15 Pct Recovery = 96% Analysis Date = 11/16/15 Pct Recovery = 96% Analysis Date = 11/12/15 Pct Recovery = 96% Analysis Date = 11/12/15 Pct Recovery = 96% Analysis Date = 11/07/15 Pct Recovery = 96% Analysis Date = 11/07/15 Pct Recovery = 96% Analysis Date = 11/02/15 Pct Recovery = 96% Analysis Date = 11/02/15 Pct Recovery = 96% Analysis Date = 10/28/15 Pct Recovery = 96% Analysis Date = 10/28/15 Pct Recovery = 96% Analysis Date = 10/24/15 Pct Recovery = 96% Analysis Date = 10/24/15 Pct Recovery = 96% Analysis Date = 10/19/15 Pct Recovery = 96% Analysis Date = 10/19/15 Pct Recovery = 96% Analysis Date = 10/14/15 Pct Recovery = 96% Analysis Date = 10/14/15 Pct Recovery = 96% Analysis Date = 10/09/15 Pct Recovery = 96% Analysis Date = 10/09/15 Pct Recovery = 96% Analysis Date = 10/04/15 Pct Recovery = 96% Analysis Date = 10/04/15 Pct Recovery = 96% Analysis Date = 09/30/15 Pct Recovery = 96% Analysis Date = 09/30/15 Pct Recovery = 96% Analysis Date = 09/25/15 Pct Recovery = 96% Analysis Date = 09/25/15 Pct Recovery = 96% Analysis Date = 09/20/15 Pct Recovery = 96% Analysis Date = 09/20/15 Pct Recovery = 96% Analysis Date = 09/15/15 Pct Recovery = 96% Analysis Date = 09/15/15 Pct Recovery = 96% Analysis Date = 09/11/15 Pct Recovery = 96% Analysis Date = 09/11/15 Pct Recovery = 96% Analysis Date = 09/06/15 Pct Recovery = 96% Analysis Date = 09/06/15 Pct Recovery = 96% Analysis Date = 09/01/15 Pct Recovery = 96% Analysis Date = 09/01/15 Pct Recovery = 96% Analysis Date = 08/27/15 Pct Recovery = 96% Analysis Date = 08/27/15 Pct Recovery = 96% Analysis Date = 08/23/15 Pct Recovery = 96% Analysis Date = 08/23/15 Pct Recovery = 96% Analysis Date = 08/18/15 Pct Recovery = 96% Analysis Date = 08/18/15 Pct Recovery = 96% Analysis Date = 08/13/15 Pct Recovery = 96% Analysis Date = 08/13/15 Pct Recovery = 96% Analysis Date = 08/08/15 Pct Recovery = 96% Analysis Date = 08/08/15 Pct Recovery = 96% Analysis Date = 08/03/15 Pct Recovery = 96% Analysis Date = 08/03/15 Pct Recovery = 96% Analysis Date = 07/30/15 Pct Recovery = 96% Analysis Date = 07/30/15 Pct Recovery = 96% Analysis Date = 07/25/15 Pct Recovery = 96% Analysis Date = 07/25/15 Pct Recovery = 96% Analysis Date = 07/20/15 Pct Recovery = 96% Analysis Date = 07/20/15 Pct Recovery = 96% Analysis Date = 07/15/15 Pct Recovery = 96% Analysis Date = 07/15/15 Pct Recovery = 96% Analysis Date = 07/11/15 Pct Recovery = 96% Analysis Date = 07/11/15 Pct Recovery = 96% Analysis Date = 07/06/15 Pct Recovery = 96% Analysis Date = 07/06/15 Pct Recovery = 96% Analysis Date = 07/01/15 Pct Recovery = 96% Analysis Date = 07/01/15 Pct Recovery = 96% Analysis Date = 06/26/15 Pct Recovery = 96% Analysis Date = 06/26/15 Pct Recovery = 96% Analysis Date = 06/21/15 Pct Recovery = 96% Analysis Date = 06/21/15 Pct Recovery = 96% Analysis Date = 06/17/15 Pct Recovery = 96% Analysis Date = 06/17/15 Pct Recovery = 96% Analysis Date = 06/12/15 Pct Recovery = 96% Analysis Date = 06/12/15 Pct Recovery = 96% Analysis Date = 06/07/15 Pct Recovery = 96% Analysis Date = 06/07/15 Pct Recovery = 96% Analysis Date = 06/02/15 Pct Recovery = 96% Analysis Date = 06/02/15 Pct Recovery = 96% Analysis Date = 05/29/15 Pct Recovery = 96% Analysis Date = 05/29/15 Pct Recovery = 96% Analysis Date = 05/24/15 Pct Recovery = 96% Analysis Date = 05/24/15 Pct Recovery = 96% Analysis Date = 05/19/15 Pct Recovery = 96% Analysis Date = 05/19/15 Pct Recovery = 96% Analysis Date = 05/14/15 Pct Recovery = 96% Analysis Date = 05/14/15 Pct Recovery = 96% Analysis Date = 05/10/15 Pct Recovery = 96% Analysis Date = 05/10/15 Pct Recovery = 96% Analysis Date = 05/05/15 Pct Recovery = 97% Analysis Date = 05/05/15 Pct Recovery = 97% Analysis Date = 04/30/15 Pct Recovery = 97% Analysis Date = 04/30/15 Pct Recovery = 97% Analysis Date = 04/25/15 Pct Recovery = 97% Analysis Date = 04/25/15 Pct Recovery = 97% Analysis Date = 04/20/15 Pct Recovery = 97% Analysis Date = 04/20/15 Pct Recovery = 97% Analysis Date = 04/16/15 Pct Recovery = 97% Analysis Date = 04/16/15 Pct Recovery = 97% Analysis Date = 04/11/15 Pct Recovery = 97% Analysis Date = 04/11/15 Pct Recovery = 97% Analysis Date = 04/06/15 Pct Recovery = 98% Analysis Date = 04/06/15 Pct Recovery = 98% Analysis Date = 04/01/15 Pct Recovery = 98% Analysis Date = 04/01/15 Pct Recovery = 98% Analysis Date = 03/28/15 Pct Recovery = 98% Analysis Date = 03/28/15 Pct Recovery = 98% Analysis Date = 03/23/15 Pct Recovery = 98% Analysis Date = 03/23/15 Pct Recovery = 98% Analysis Date = 03/18/15 Pct Recovery = 98% Analysis Date = 03/18/15 Pct Recovery = 98% Analysis Date = 03/13/15 Pct Recovery = 98% Analysis Date = 03/13/15 Pct Recovery = 98% Analysis Date = 03/09/15 Pct Recovery = 99% Analysis Date = 03/09/15 Pct Recovery = 99% Analysis Date = 03/04/15 Pct Recovery = 99% Analysis Date = 03/04/15 Pct Recovery = 99% Analysis Date = 02/27/15 Pct Recovery = 99% Analysis Date = 02/27/15 Pct Recovery = 99% Analysis Date = 02/22/15 Pct Recovery = 99% Analysis Date = 02/22/15 Pct Recovery = 99% Analysis Date = 02/17/15 Pct Recovery = 99% Analysis Date = 02/17/15 Pct Recovery = 99% Analysis Date = 02/13/15 Pct Recovery = 99% Analysis Date = 02/13/15 Pct Recovery = 99% Analysis Date = 02/08/15 Pct Recovery = 100% Analysis Date = 02/08/15 Pct Recovery = 100% Analysis Date = 02/03/15 Pct Recovery = 100% Analysis Date = 02/03/15 Pct Recovery = 100% Analysis Date = 01/29/15 Pct Recovery = 100% Analysis Date = 01/29/15 Pct Recovery = 100% Analysis Date = 01/25/15 Pct Recovery = 100% Analysis Date = 01/25/15 Pct Recovery = 100% Analysis Date = 01/20/15 Pct Recovery = 100% Analysis Date = 01/20/15 Pct Recovery = 100% Analysis Date = 01/15/15 Pct Recovery = 100% Analysis Date = 01/15/15 Pct Recovery = 100% Analysis Date = 01/10/15 Pct Recovery = 101% Analysis Date = 01/10/15 Pct Recovery = 101% Analysis Date = 01/06/15 Pct Recovery = 101% Analysis Date = 01/06/15 Pct Recovery = 101% Analysis Date = 01/01/15 Pct Recovery = 101% Analysis Date = 01/01/15 Pct Recovery = 101% Analysis Date = 12/27/14 Pct Recovery = 101% Analysis Date = 12/27/14 Pct Recovery = 101% Analysis Date = 12/22/14 Pct Recovery = 101% Analysis Date = 12/22/14 Pct Recovery = 101% Analysis Date = 12/17/14 Pct Recovery = 101% Analysis Date = 12/17/14 Pct Recovery = 101% Analysis Date = 12/13/14 Pct Recovery = 102% Analysis Date = 12/13/14 Pct Recovery = 102% Analysis Date = 12/08/14 Pct Recovery = 102% Analysis Date = 12/08/14 Pct Recovery = 102% Analysis Date = 12/03/14 Pct Recovery = 102% Analysis Date = 12/03/14 Pct Recovery = 102% Analysis Date = 11/28/14 Pct Recovery = 102% Analysis Date = 11/28/14 Pct Recovery = 102% Analysis Date = 11/24/14 Pct Recovery = 102% Analysis Date = 11/24/14 Pct Recovery = 102% Analysis Date = 11/19/14 Pct Recovery = 103% Analysis Date = 11/19/14 Pct Recovery = 103% Analysis Date = 11/14/14 Pct Recovery = 103% Analysis Date = 11/14/14 Pct Recovery = 103% Analysis Date = 11/09/14 Pct Recovery = 103% Analysis Date = 11/09/14 Pct Recovery = 103% Analysis Date = 11/05/14 Pct Recovery = 103% Analysis Date = 11/05/14 Pct Recovery = 103% Analysis Date = 10/31/14 Pct Recovery = 103% Analysis Date = 10/31/14 Pct Recovery = 103% Analysis Date = 10/26/14 Pct Recovery = 103% Analysis Date = 10/26/14 Pct Recovery = 103% Analysis Date = 10/21/14 Pct Recovery = 104% Analysis Date = 10/21/14 Pct Recovery = 104% Analysis Date = 10/16/14 Pct Recovery = 104% Analysis Date = 10/16/14 Pct Recovery = 104% Analysis Date = 10/12/14 Pct Recovery = 104% Analysis Date = 10/12/14 Pct Recovery = 104% Analysis Date = 10/07/14 Pct Recovery = 104% Analysis Date = 10/07/14 Pct Recovery = 104% Analysis Date = 10/02/14 Pct Recovery = 104% Analysis Date = 10/02/14 Pct Recovery = 104% Analysis Date = 09/27/14 Pct Recovery = 105% Analysis Date = 09/27/14 Pct Recovery = 105% Analysis Date = 09/23/14 Pct Recovery = 105% Analysis Date = 09/23/14 Pct Recovery = 105% Analysis Date = 09/18/14 Pct Recovery = 105% Analysis Date = 09/18/14 Pct Recovery = 105% Analysis Date = 09/13/14 Pct Recovery = 105% Analysis Date = 09/13/14 Pct Recovery = 105% Analysis Date = 09/08/14 Pct Recovery = 105% Analysis Date = 09/08/14 Pct Recovery = 105% Analysis Date = 09/04/14 Pct Recovery = 105% Analysis Date = 09/04/14 Pct Recovery = 105% Analysis Date = 08/30/14 Pct Recovery = 106% Analysis Date = 08/30/14 Pct Recovery = 106% Analysis Date = 08/25/14 Pct Recovery = 106% Analysis Date = 08/25/14 Pct Recovery = 106% Analysis Date = 08/20/14 Pct Recovery = 106% Analysis Date = 08/20/14 Pct Recovery = 106% Analysis Date = 08/15/14 Pct Recovery = 106% Analysis Date = 08/15/14 Pct Recovery = 106% Analysis Date = 08/11/14 Pct Recovery = 106% Analysis Date = 08/11/14 Pct Recovery = 106% Analysis Date = 08/06/14 Pct Recovery = 107% Analysis Date = 08/06/14 Pct Recovery = 107% Analysis Date = 08/01/14 Pct Recovery = 107% Analysis Date = 08/01/14 Pct Recovery = 107% Analysis Date = 07/27/14 Pct Recovery = 107% Analysis Date = 07/27/14 Pct Recovery = 107% Analysis Date = 07/23/14 Pct Recovery = 107% Analysis Date = 07/23/14 Pct Recovery = 107% Analysis Date = 07/18/14 Pct Recovery = 107% Analysis Date = 07/18/14 Pct Recovery = 107% Analysis Date = 07/13/14 Pct Recovery = 108% Analysis Date = 07/13/14 Pct Recovery = 108% Analysis Date = 07/08/14 Pct Recovery = 108% Analysis Date = 07/08/14 Pct Recovery = 108% Analysis Date = 07/04/14 Pct Recovery = 108% Analysis Date = 07/04/14 Pct Recovery = 108% Analysis Date = 06/29/14 Pct Recovery = 108% Analysis Date = 06/29/14 Pct Recovery = 108% Analysis Date = 06/24/14 Pct Recovery = 108% Analysis Date = 06/24/14 Pct Recovery = 108% Analysis Date = 06/19/14 Pct Recovery = 108% Analysis Date = 06/19/14 Pct Recovery = 108% Analysis Date = 06/14/14 Pct Recovery = 109% Analysis Date = 06/14/14 Pct Recovery = 109% Analysis Date = 06/10/14 Pct Recovery = 109% Analysis Date = 06/10/14 Pct Recovery = 109% Analysis Date = 06/05/14 Pct Recovery = 109% Analysis Date = 06/05/14 Pct Recovery = 109% Analysis Date = 05/31/14 Pct Recovery = 109% Analysis Date = 05/31/14 Pct Recovery = 109% Analysis Date = 05/26/14 Pct Recovery = 109% Analysis Date = 05/26/14 Pct Recovery = 109% Analysis Date = 05/22/14 Pct Recovery = 110% Analysis Date = 05/22/14 Pct Recovery = 110% Analysis Date = 05/17/14 Pct Recovery = 110% Analysis Date = 05/17/14 Pct Recovery = 110% Analysis Date = 05/12/14 Pct Recovery = 110% Analysis Date = 05/12/14 Pct Recovery = 110% Analysis Date = 05/07/14 Pct Recovery = 110% Analysis Date = 05/07/14 Pct Recovery = 110% Analysis Date = 05/03/14 Pct Recovery = 110% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
2-HEXANONE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 6 97% 13% 97% 14%
>= Reporting Level 37 100% 11% 99% 10%
Total 43 100% 11% 99% 12%

Sample Statistics
2-HEXANONE

Characteristic N % % Basis
Plotted 43 100% Spiked
Estimated Values 1 2% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 43 .  
False Negatives 0 0% 0 out of 43
Not Spiked 23 .  
False Positives 0 0% 0 out of 23

BQS OBSP Determination:
3-CHLOROPROPENE
METHOD: 4440 , TESTIDCODE: 78109GCM66
Open Data Set

Analysis Date = 08/04/16 SpikeMix = Crescent 03FF058: 40 µl & Supelco LC20141V: 40 µl Pct Recovery = 98% Analysis Date = 07/20/16 SpikeMix = Supelco LC20141V: 40 µl & Accu 216041125: 40 µl Pct Recovery = 89% Analysis Date = 11/21/16 SpikeMix = Crescent 03FF058: 25 µl & Supelco LC20141V: 25 µl Pct Recovery = 87% Analysis Date = 09/08/16 SpikeMix = Supelco LC20141V: 25 µl & Accu 216041125: 25 µl Pct Recovery = 91% Analysis Date = 03/06/15 SpikeMix = ERA 0227-14-06.1A: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 97% Analysis Date = 12/17/14 SpikeMix = Supelco LC06438: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 94% Analysis Date = 09/21/14 SpikeMix = Supelco LC06438: 20 µl Pct Recovery = 103% Analysis Date = 06/10/14 SpikeMix = NSI 032614: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 113% Analysis Date = 03/19/15 SpikeMix = Spex Organics C1140417015: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 104% Analysis Date = 11/22/14 SpikeMix = NSI 032614: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 102% Analysis Date = 08/19/14 SpikeMix = Spex Organics C1140417015: 20 µl & Accu 214031115: 20 µl Pct Recovery = 100% Analysis Date = 08/16/14 SpikeMix = ERA 0227-14-06.1A: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 102% Analysis Date = 09/29/15 SpikeMix = Accu 215041380: 25 µl & ERA 0406-15-03: 25 µl Pct Recovery = 81% Analysis Date = 08/15/15 SpikeMix = Supelco LC13545: 25 µl & Crescent 04EE008: 25 µl Pct Recovery = 84% Analysis Date = 07/13/15 SpikeMix = Crescent 04EE008: 25 µl & NSI 050515AVOC: 25 µl Pct Recovery = 94% Analysis Date = 10/13/16 SpikeMix = NSI 041816AVOC: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 106% Analysis Date = 05/27/16 SpikeMix = Phenova B20160319: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 87% Analysis Date = 04/02/16 SpikeMix = Supelco LC13545: 15 µl & Accu 215041380: 15 µl Pct Recovery = 91% Analysis Date = 03/04/16 SpikeMix = Accu 215041380: 15 µl & ERA 0406-15-03: 15 µl Pct Recovery = 97% Analysis Date = 06/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Accu 215041380: 15 µl Pct Recovery = 94% Analysis Date = 12/18/15 SpikeMix = Supelco LC13545: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 90% Analysis Date = 10/17/15 SpikeMix = Crescent 04EE008: 15 µl & NSI 050515AVOC: 15 µl Pct Recovery = 88% Analysis Date = 05/09/15 SpikeMix = Spex Organics EN150428007: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 96% Analysis Date = 10/21/14 SpikeMix = ERA 0227-14-06.1A: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 100% Analysis Date = 06/18/14 SpikeMix = Supelco LC06438: 10 µl & Accu 214031115: 10 µl Pct Recovery = 113% Analysis Date = 05/30/14 SpikeMix = NSI 032614: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 110% Analysis Date = 05/03/14 SpikeMix = Crescent 03DD004: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 105% Analysis Date = 11/06/14 SpikeMix = Spex Organics C1140417015: 10 µl & Crescent 03DD004: 10 µl Pct Recovery = 92% Analysis Date = 09/09/14 SpikeMix = NSI 032614: 10 µl & Spex Organics C1140417015: 10 µl Pct Recovery = 111% Analysis Date = 07/23/14 SpikeMix = Spex Organics C1140417015: 10 µl & Accu 214031115: 10 µl Pct Recovery = 118% Analysis Date = 07/11/14 SpikeMix = Spex Organics C1140417015: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 104% Analysis Date = 02/18/16 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 92% Analysis Date = 11/20/15 SpikeMix = Accu 215041380: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 90% Analysis Date = 11/12/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 93% Analysis Date = 05/21/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 92% Analysis Date = 05/13/16 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 95% Analysis Date = 01/27/16 SpikeMix = Crescent 04EE008: 10 µl & NSI 050515AVOC: 10 µl Pct Recovery = 93% Analysis Date = 07/31/15 SpikeMix = Crescent 04EE008: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 80% Analysis Date = 05/09/15 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 104% Analysis Date = 11/21/16 Pct Recovery = 95% Analysis Date = 11/16/16 Pct Recovery = 95% Analysis Date = 11/16/16 Pct Recovery = 95% Analysis Date = 11/11/16 Pct Recovery = 95% Analysis Date = 11/11/16 Pct Recovery = 95% Analysis Date = 11/07/16 Pct Recovery = 95% Analysis Date = 11/07/16 Pct Recovery = 95% Analysis Date = 11/02/16 Pct Recovery = 95% Analysis Date = 11/02/16 Pct Recovery = 95% Analysis Date = 10/28/16 Pct Recovery = 95% Analysis Date = 10/28/16 Pct Recovery = 95% Analysis Date = 10/24/16 Pct Recovery = 95% Analysis Date = 10/24/16 Pct Recovery = 95% Analysis Date = 10/19/16 Pct Recovery = 94% Analysis Date = 10/19/16 Pct Recovery = 94% Analysis Date = 10/14/16 Pct Recovery = 94% Analysis Date = 10/14/16 Pct Recovery = 94% Analysis Date = 10/10/16 Pct Recovery = 94% Analysis Date = 10/10/16 Pct Recovery = 94% Analysis Date = 10/05/16 Pct Recovery = 94% Analysis Date = 10/05/16 Pct Recovery = 94% Analysis Date = 09/30/16 Pct Recovery = 94% Analysis Date = 09/30/16 Pct Recovery = 94% Analysis Date = 09/26/16 Pct Recovery = 94% Analysis Date = 09/26/16 Pct Recovery = 94% Analysis Date = 09/21/16 Pct Recovery = 94% Analysis Date = 09/21/16 Pct Recovery = 94% Analysis Date = 09/16/16 Pct Recovery = 94% Analysis Date = 09/16/16 Pct Recovery = 94% Analysis Date = 09/12/16 Pct Recovery = 94% Analysis Date = 09/12/16 Pct Recovery = 94% Analysis Date = 09/07/16 Pct Recovery = 94% Analysis Date = 09/07/16 Pct Recovery = 94% Analysis Date = 09/02/16 Pct Recovery = 94% Analysis Date = 09/02/16 Pct Recovery = 94% Analysis Date = 08/29/16 Pct Recovery = 94% Analysis Date = 08/29/16 Pct Recovery = 94% Analysis Date = 08/24/16 Pct Recovery = 94% Analysis Date = 08/24/16 Pct Recovery = 94% Analysis Date = 08/19/16 Pct Recovery = 94% Analysis Date = 08/19/16 Pct Recovery = 94% Analysis Date = 08/15/16 Pct Recovery = 94% Analysis Date = 08/15/16 Pct Recovery = 94% Analysis Date = 08/10/16 Pct Recovery = 94% Analysis Date = 08/10/16 Pct Recovery = 94% Analysis Date = 08/05/16 Pct Recovery = 94% Analysis Date = 08/05/16 Pct Recovery = 94% Analysis Date = 08/01/16 Pct Recovery = 94% Analysis Date = 08/01/16 Pct Recovery = 94% Analysis Date = 07/27/16 Pct Recovery = 94% Analysis Date = 07/27/16 Pct Recovery = 94% Analysis Date = 07/22/16 Pct Recovery = 93% Analysis Date = 07/22/16 Pct Recovery = 93% Analysis Date = 07/18/16 Pct Recovery = 93% Analysis Date = 07/18/16 Pct Recovery = 93% Analysis Date = 07/13/16 Pct Recovery = 93% Analysis Date = 07/13/16 Pct Recovery = 93% Analysis Date = 07/08/16 Pct Recovery = 93% Analysis Date = 07/08/16 Pct Recovery = 93% Analysis Date = 07/04/16 Pct Recovery = 93% Analysis Date = 07/04/16 Pct Recovery = 93% Analysis Date = 06/29/16 Pct Recovery = 93% Analysis Date = 06/29/16 Pct Recovery = 93% Analysis Date = 06/24/16 Pct Recovery = 93% Analysis Date = 06/24/16 Pct Recovery = 93% Analysis Date = 06/20/16 Pct Recovery = 93% Analysis Date = 06/20/16 Pct Recovery = 93% Analysis Date = 06/15/16 Pct Recovery = 93% Analysis Date = 06/15/16 Pct Recovery = 93% Analysis Date = 06/10/16 Pct Recovery = 93% Analysis Date = 06/10/16 Pct Recovery = 93% Analysis Date = 06/06/16 Pct Recovery = 93% Analysis Date = 06/06/16 Pct Recovery = 93% Analysis Date = 06/01/16 Pct Recovery = 93% Analysis Date = 06/01/16 Pct Recovery = 93% Analysis Date = 05/27/16 Pct Recovery = 93% Analysis Date = 05/27/16 Pct Recovery = 93% Analysis Date = 05/23/16 Pct Recovery = 93% Analysis Date = 05/23/16 Pct Recovery = 93% Analysis Date = 05/18/16 Pct Recovery = 93% Analysis Date = 05/18/16 Pct Recovery = 93% Analysis Date = 05/13/16 Pct Recovery = 93% Analysis Date = 05/13/16 Pct Recovery = 93% Analysis Date = 05/09/16 Pct Recovery = 92% Analysis Date = 05/09/16 Pct Recovery = 92% Analysis Date = 05/04/16 Pct Recovery = 92% Analysis Date = 05/04/16 Pct Recovery = 92% Analysis Date = 04/29/16 Pct Recovery = 92% Analysis Date = 04/29/16 Pct Recovery = 92% Analysis Date = 04/25/16 Pct Recovery = 92% Analysis Date = 04/25/16 Pct Recovery = 92% Analysis Date = 04/20/16 Pct Recovery = 92% Analysis Date = 04/20/16 Pct Recovery = 92% Analysis Date = 04/15/16 Pct Recovery = 92% Analysis Date = 04/15/16 Pct Recovery = 92% Analysis Date = 04/11/16 Pct Recovery = 92% Analysis Date = 04/11/16 Pct Recovery = 92% Analysis Date = 04/06/16 Pct Recovery = 92% Analysis Date = 04/06/16 Pct Recovery = 92% Analysis Date = 04/01/16 Pct Recovery = 92% Analysis Date = 04/01/16 Pct Recovery = 92% Analysis Date = 03/28/16 Pct Recovery = 92% Analysis Date = 03/28/16 Pct Recovery = 92% Analysis Date = 03/23/16 Pct Recovery = 92% Analysis Date = 03/23/16 Pct Recovery = 92% Analysis Date = 03/18/16 Pct Recovery = 92% Analysis Date = 03/18/16 Pct Recovery = 92% Analysis Date = 03/14/16 Pct Recovery = 92% Analysis Date = 03/14/16 Pct Recovery = 92% Analysis Date = 03/09/16 Pct Recovery = 91% Analysis Date = 03/09/16 Pct Recovery = 91% Analysis Date = 03/04/16 Pct Recovery = 91% Analysis Date = 03/04/16 Pct Recovery = 91% Analysis Date = 02/29/16 Pct Recovery = 91% Analysis Date = 02/29/16 Pct Recovery = 91% Analysis Date = 02/24/16 Pct Recovery = 91% Analysis Date = 02/24/16 Pct Recovery = 91% Analysis Date = 02/19/16 Pct Recovery = 91% Analysis Date = 02/19/16 Pct Recovery = 91% Analysis Date = 02/15/16 Pct Recovery = 91% Analysis Date = 02/15/16 Pct Recovery = 91% Analysis Date = 02/10/16 Pct Recovery = 91% Analysis Date = 02/10/16 Pct Recovery = 91% Analysis Date = 02/05/16 Pct Recovery = 91% Analysis Date = 02/05/16 Pct Recovery = 91% Analysis Date = 02/01/16 Pct Recovery = 91% Analysis Date = 02/01/16 Pct Recovery = 91% Analysis Date = 01/27/16 Pct Recovery = 91% Analysis Date = 01/27/16 Pct Recovery = 91% Analysis Date = 01/22/16 Pct Recovery = 91% Analysis Date = 01/22/16 Pct Recovery = 91% Analysis Date = 01/18/16 Pct Recovery = 91% Analysis Date = 01/18/16 Pct Recovery = 91% Analysis Date = 01/13/16 Pct Recovery = 91% Analysis Date = 01/13/16 Pct Recovery = 91% Analysis Date = 01/08/16 Pct Recovery = 91% Analysis Date = 01/08/16 Pct Recovery = 91% Analysis Date = 01/04/16 Pct Recovery = 91% Analysis Date = 01/04/16 Pct Recovery = 91% Analysis Date = 12/30/15 Pct Recovery = 91% Analysis Date = 12/30/15 Pct Recovery = 91% Analysis Date = 12/25/15 Pct Recovery = 90% Analysis Date = 12/25/15 Pct Recovery = 90% Analysis Date = 12/21/15 Pct Recovery = 90% Analysis Date = 12/21/15 Pct Recovery = 90% Analysis Date = 12/16/15 Pct Recovery = 90% Analysis Date = 12/16/15 Pct Recovery = 90% Analysis Date = 12/11/15 Pct Recovery = 90% Analysis Date = 12/11/15 Pct Recovery = 90% Analysis Date = 12/07/15 Pct Recovery = 90% Analysis Date = 12/07/15 Pct Recovery = 90% Analysis Date = 12/02/15 Pct Recovery = 90% Analysis Date = 12/02/15 Pct Recovery = 90% Analysis Date = 11/27/15 Pct Recovery = 91% Analysis Date = 11/27/15 Pct Recovery = 91% Analysis Date = 11/23/15 Pct Recovery = 91% Analysis Date = 11/23/15 Pct Recovery = 91% Analysis Date = 11/18/15 Pct Recovery = 91% Analysis Date = 11/18/15 Pct Recovery = 91% Analysis Date = 11/13/15 Pct Recovery = 91% Analysis Date = 11/13/15 Pct Recovery = 91% Analysis Date = 11/09/15 Pct Recovery = 91% Analysis Date = 11/09/15 Pct Recovery = 91% Analysis Date = 11/04/15 Pct Recovery = 91% Analysis Date = 11/04/15 Pct Recovery = 91% Analysis Date = 10/30/15 Pct Recovery = 91% Analysis Date = 10/30/15 Pct Recovery = 91% Analysis Date = 10/26/15 Pct Recovery = 91% Analysis Date = 10/26/15 Pct Recovery = 91% Analysis Date = 10/21/15 Pct Recovery = 91% Analysis Date = 10/21/15 Pct Recovery = 91% Analysis Date = 10/16/15 Pct Recovery = 91% Analysis Date = 10/16/15 Pct Recovery = 91% Analysis Date = 10/12/15 Pct Recovery = 91% Analysis Date = 10/12/15 Pct Recovery = 91% Analysis Date = 10/07/15 Pct Recovery = 91% Analysis Date = 10/07/15 Pct Recovery = 91% Analysis Date = 10/02/15 Pct Recovery = 91% Analysis Date = 10/02/15 Pct Recovery = 91% Analysis Date = 09/28/15 Pct Recovery = 91% Analysis Date = 09/28/15 Pct Recovery = 91% Analysis Date = 09/23/15 Pct Recovery = 91% Analysis Date = 09/23/15 Pct Recovery = 91% Analysis Date = 09/18/15 Pct Recovery = 91% Analysis Date = 09/18/15 Pct Recovery = 91% Analysis Date = 09/14/15 Pct Recovery = 91% Analysis Date = 09/14/15 Pct Recovery = 91% Analysis Date = 09/09/15 Pct Recovery = 91% Analysis Date = 09/09/15 Pct Recovery = 91% Analysis Date = 09/04/15 Pct Recovery = 91% Analysis Date = 09/04/15 Pct Recovery = 91% Analysis Date = 08/31/15 Pct Recovery = 91% Analysis Date = 08/31/15 Pct Recovery = 91% Analysis Date = 08/26/15 Pct Recovery = 91% Analysis Date = 08/26/15 Pct Recovery = 91% Analysis Date = 08/21/15 Pct Recovery = 91% Analysis Date = 08/21/15 Pct Recovery = 91% Analysis Date = 08/17/15 Pct Recovery = 92% Analysis Date = 08/17/15 Pct Recovery = 92% Analysis Date = 08/12/15 Pct Recovery = 92% Analysis Date = 08/12/15 Pct Recovery = 92% Analysis Date = 08/07/15 Pct Recovery = 92% Analysis Date = 08/07/15 Pct Recovery = 92% Analysis Date = 08/03/15 Pct Recovery = 92% Analysis Date = 08/03/15 Pct Recovery = 92% Analysis Date = 07/29/15 Pct Recovery = 92% Analysis Date = 07/29/15 Pct Recovery = 92% Analysis Date = 07/24/15 Pct Recovery = 92% Analysis Date = 07/24/15 Pct Recovery = 92% Analysis Date = 07/20/15 Pct Recovery = 92% Analysis Date = 07/20/15 Pct Recovery = 92% Analysis Date = 07/15/15 Pct Recovery = 92% Analysis Date = 07/15/15 Pct Recovery = 92% Analysis Date = 07/10/15 Pct Recovery = 92% Analysis Date = 07/10/15 Pct Recovery = 92% Analysis Date = 07/06/15 Pct Recovery = 92% Analysis Date = 07/06/15 Pct Recovery = 92% Analysis Date = 07/01/15 Pct Recovery = 93% Analysis Date = 07/01/15 Pct Recovery = 93% Analysis Date = 06/26/15 Pct Recovery = 93% Analysis Date = 06/26/15 Pct Recovery = 93% Analysis Date = 06/22/15 Pct Recovery = 93% Analysis Date = 06/22/15 Pct Recovery = 93% Analysis Date = 06/17/15 Pct Recovery = 93% Analysis Date = 06/17/15 Pct Recovery = 93% Analysis Date = 06/12/15 Pct Recovery = 93% Analysis Date = 06/12/15 Pct Recovery = 93% Analysis Date = 06/08/15 Pct Recovery = 93% Analysis Date = 06/08/15 Pct Recovery = 93% Analysis Date = 06/03/15 Pct Recovery = 93% Analysis Date = 06/03/15 Pct Recovery = 93% Analysis Date = 05/29/15 Pct Recovery = 93% Analysis Date = 05/29/15 Pct Recovery = 93% Analysis Date = 05/25/15 Pct Recovery = 94% Analysis Date = 05/25/15 Pct Recovery = 94% Analysis Date = 05/20/15 Pct Recovery = 94% Analysis Date = 05/20/15 Pct Recovery = 94% Analysis Date = 05/15/15 Pct Recovery = 94% Analysis Date = 05/15/15 Pct Recovery = 94% Analysis Date = 05/11/15 Pct Recovery = 94% Analysis Date = 05/11/15 Pct Recovery = 94% Analysis Date = 05/06/15 Pct Recovery = 94% Analysis Date = 05/06/15 Pct Recovery = 94% Analysis Date = 05/01/15 Pct Recovery = 94% Analysis Date = 05/01/15 Pct Recovery = 94% Analysis Date = 04/27/15 Pct Recovery = 95% Analysis Date = 04/27/15 Pct Recovery = 95% Analysis Date = 04/22/15 Pct Recovery = 95% Analysis Date = 04/22/15 Pct Recovery = 95% Analysis Date = 04/17/15 Pct Recovery = 95% Analysis Date = 04/17/15 Pct Recovery = 95% Analysis Date = 04/13/15 Pct Recovery = 95% Analysis Date = 04/13/15 Pct Recovery = 95% Analysis Date = 04/08/15 Pct Recovery = 95% Analysis Date = 04/08/15 Pct Recovery = 95% Analysis Date = 04/03/15 Pct Recovery = 95% Analysis Date = 04/03/15 Pct Recovery = 95% Analysis Date = 03/30/15 Pct Recovery = 96% Analysis Date = 03/30/15 Pct Recovery = 96% Analysis Date = 03/25/15 Pct Recovery = 96% Analysis Date = 03/25/15 Pct Recovery = 96% Analysis Date = 03/20/15 Pct Recovery = 96% Analysis Date = 03/20/15 Pct Recovery = 96% Analysis Date = 03/16/15 Pct Recovery = 96% Analysis Date = 03/16/15 Pct Recovery = 96% Analysis Date = 03/11/15 Pct Recovery = 96% Analysis Date = 03/11/15 Pct Recovery = 96% Analysis Date = 03/06/15 Pct Recovery = 97% Analysis Date = 03/06/15 Pct Recovery = 97% Analysis Date = 03/02/15 Pct Recovery = 97% Analysis Date = 03/02/15 Pct Recovery = 97% Analysis Date = 02/25/15 Pct Recovery = 97% Analysis Date = 02/25/15 Pct Recovery = 97% Analysis Date = 02/20/15 Pct Recovery = 97% Analysis Date = 02/20/15 Pct Recovery = 97% Analysis Date = 02/16/15 Pct Recovery = 97% Analysis Date = 02/16/15 Pct Recovery = 97% Analysis Date = 02/11/15 Pct Recovery = 98% Analysis Date = 02/11/15 Pct Recovery = 98% Analysis Date = 02/06/15 Pct Recovery = 98% Analysis Date = 02/06/15 Pct Recovery = 98% Analysis Date = 02/02/15 Pct Recovery = 98% Analysis Date = 02/02/15 Pct Recovery = 98% Analysis Date = 01/28/15 Pct Recovery = 98% Analysis Date = 01/28/15 Pct Recovery = 98% Analysis Date = 01/23/15 Pct Recovery = 99% Analysis Date = 01/23/15 Pct Recovery = 99% Analysis Date = 01/19/15 Pct Recovery = 99% Analysis Date = 01/19/15 Pct Recovery = 99% Analysis Date = 01/14/15 Pct Recovery = 99% Analysis Date = 01/14/15 Pct Recovery = 99% Analysis Date = 01/09/15 Pct Recovery = 99% Analysis Date = 01/09/15 Pct Recovery = 99% Analysis Date = 01/05/15 Pct Recovery = 99% Analysis Date = 01/05/15 Pct Recovery = 99% Analysis Date = 12/31/14 Pct Recovery = 100% Analysis Date = 12/31/14 Pct Recovery = 100% Analysis Date = 12/26/14 Pct Recovery = 100% Analysis Date = 12/26/14 Pct Recovery = 100% Analysis Date = 12/22/14 Pct Recovery = 100% Analysis Date = 12/22/14 Pct Recovery = 100% Analysis Date = 12/17/14 Pct Recovery = 100% Analysis Date = 12/17/14 Pct Recovery = 100% Analysis Date = 12/12/14 Pct Recovery = 101% Analysis Date = 12/12/14 Pct Recovery = 101% Analysis Date = 12/08/14 Pct Recovery = 101% Analysis Date = 12/08/14 Pct Recovery = 101% Analysis Date = 12/03/14 Pct Recovery = 101% Analysis Date = 12/03/14 Pct Recovery = 101% Analysis Date = 11/28/14 Pct Recovery = 101% Analysis Date = 11/28/14 Pct Recovery = 101% Analysis Date = 11/24/14 Pct Recovery = 101% Analysis Date = 11/24/14 Pct Recovery = 101% Analysis Date = 11/19/14 Pct Recovery = 102% Analysis Date = 11/19/14 Pct Recovery = 102% Analysis Date = 11/14/14 Pct Recovery = 102% Analysis Date = 11/14/14 Pct Recovery = 102% Analysis Date = 11/10/14 Pct Recovery = 102% Analysis Date = 11/10/14 Pct Recovery = 102% Analysis Date = 11/05/14 Pct Recovery = 102% Analysis Date = 11/05/14 Pct Recovery = 102% Analysis Date = 10/31/14 Pct Recovery = 102% Analysis Date = 10/31/14 Pct Recovery = 102% Analysis Date = 10/27/14 Pct Recovery = 103% Analysis Date = 10/27/14 Pct Recovery = 103% Analysis Date = 10/22/14 Pct Recovery = 103% Analysis Date = 10/22/14 Pct Recovery = 103% Analysis Date = 10/17/14 Pct Recovery = 103% Analysis Date = 10/17/14 Pct Recovery = 103% Analysis Date = 10/13/14 Pct Recovery = 103% Analysis Date = 10/13/14 Pct Recovery = 103% Analysis Date = 10/08/14 Pct Recovery = 103% Analysis Date = 10/08/14 Pct Recovery = 103% Analysis Date = 10/03/14 Pct Recovery = 104% Analysis Date = 10/03/14 Pct Recovery = 104% Analysis Date = 09/29/14 Pct Recovery = 104% Analysis Date = 09/29/14 Pct Recovery = 104% Analysis Date = 09/24/14 Pct Recovery = 104% Analysis Date = 09/24/14 Pct Recovery = 104% Analysis Date = 09/19/14 Pct Recovery = 104% Analysis Date = 09/19/14 Pct Recovery = 104% Analysis Date = 09/15/14 Pct Recovery = 104% Analysis Date = 09/15/14 Pct Recovery = 104% Analysis Date = 09/10/14 Pct Recovery = 105% Analysis Date = 09/10/14 Pct Recovery = 105% Analysis Date = 09/05/14 Pct Recovery = 105% Analysis Date = 09/05/14 Pct Recovery = 105% Analysis Date = 09/01/14 Pct Recovery = 105% Analysis Date = 09/01/14 Pct Recovery = 105% Analysis Date = 08/27/14 Pct Recovery = 105% Analysis Date = 08/27/14 Pct Recovery = 105% Analysis Date = 08/22/14 Pct Recovery = 105% Analysis Date = 08/22/14 Pct Recovery = 105% Analysis Date = 08/18/14 Pct Recovery = 106% Analysis Date = 08/18/14 Pct Recovery = 106% Analysis Date = 08/13/14 Pct Recovery = 106% Analysis Date = 08/13/14 Pct Recovery = 106% Analysis Date = 08/08/14 Pct Recovery = 106% Analysis Date = 08/08/14 Pct Recovery = 106% Analysis Date = 08/04/14 Pct Recovery = 106% Analysis Date = 08/04/14 Pct Recovery = 106% Analysis Date = 07/30/14 Pct Recovery = 106% Analysis Date = 07/30/14 Pct Recovery = 106% Analysis Date = 07/25/14 Pct Recovery = 107% Analysis Date = 07/25/14 Pct Recovery = 107% Analysis Date = 07/21/14 Pct Recovery = 107% Analysis Date = 07/21/14 Pct Recovery = 107% Analysis Date = 07/16/14 Pct Recovery = 107% Analysis Date = 07/16/14 Pct Recovery = 107% Analysis Date = 07/11/14 Pct Recovery = 107% Analysis Date = 07/11/14 Pct Recovery = 107% Analysis Date = 07/07/14 Pct Recovery = 107% Analysis Date = 07/07/14 Pct Recovery = 107% Analysis Date = 07/02/14 Pct Recovery = 108% Analysis Date = 07/02/14 Pct Recovery = 108% Analysis Date = 06/27/14 Pct Recovery = 108% Analysis Date = 06/27/14 Pct Recovery = 108% Analysis Date = 06/23/14 Pct Recovery = 108% Analysis Date = 06/23/14 Pct Recovery = 108% Analysis Date = 06/18/14 Pct Recovery = 108% Analysis Date = 06/18/14 Pct Recovery = 108% Analysis Date = 06/13/14 Pct Recovery = 109% Analysis Date = 06/13/14 Pct Recovery = 109% Analysis Date = 06/09/14 Pct Recovery = 109% Analysis Date = 06/09/14 Pct Recovery = 109% Analysis Date = 06/04/14 Pct Recovery = 109% Analysis Date = 06/04/14 Pct Recovery = 109% Analysis Date = 05/30/14 Pct Recovery = 109% Analysis Date = 05/30/14 Pct Recovery = 109% Analysis Date = 05/26/14 Pct Recovery = 109% Analysis Date = 05/26/14 Pct Recovery = 109% Analysis Date = 05/21/14 Pct Recovery = 110% Analysis Date = 05/21/14 Pct Recovery = 110% Analysis Date = 05/16/14 Pct Recovery = 110% Analysis Date = 05/16/14 Pct Recovery = 110% Analysis Date = 05/12/14 Pct Recovery = 110% Analysis Date = 05/12/14 Pct Recovery = 110% Analysis Date = 05/07/14 Pct Recovery = 110% Analysis Date = 05/07/14 Pct Recovery = 110% Analysis Date = 05/03/14 Pct Recovery = 111% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
3-CHLOROPROPENE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 39 97% 9% 95% 10%
Total 39 97% 9% 95% 10%

Sample Statistics
3-CHLOROPROPENE

Characteristic N % % Basis
Plotted 39 100% Spiked
Estimated Values 39 100% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 39 .  
False Negatives 0 0% 0 out of 39
Not Spiked 34 .  
False Positives 0 0% 0 out of 34

BQS OBSP Determination:
4-CHLOROTOLUENE
METHOD: 4440 , TESTIDCODE: 77277GCM66
Open Data Set

Analysis Date = 12/12/16 SpikeMix = Accu 216041125: 40 µl & Crescent 03FF058: 40 µl Pct Recovery = 96% Analysis Date = 07/20/16 SpikeMix = Supelco LC20141V: 40 µl & Accu 216041125: 40 µl Pct Recovery = 95% Analysis Date = 07/14/16 SpikeMix = Accu 216041125: 40 µl & NSI 041816AVOC: 40 µl Pct Recovery = 82% Analysis Date = 08/12/16 SpikeMix = ChemService 5082900: 25 µl & Phenova B20160319: 25 µl Pct Recovery = 83% Analysis Date = 06/21/16 SpikeMix = Phenova B20160319: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 96% Analysis Date = 09/08/16 SpikeMix = Supelco LC20141V: 25 µl & Accu 216041125: 25 µl Pct Recovery = 76% Analysis Date = 05/24/16 SpikeMix = Accu 216041125: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 85% Analysis Date = 04/09/15 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 82% Analysis Date = 03/06/15 SpikeMix = ERA 0227-14-06.1A: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 92% Analysis Date = 11/14/14 SpikeMix = Crescent 03DD004: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 82% Analysis Date = 08/16/14 SpikeMix = ERA 0227-14-06.1A: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 84% Analysis Date = 07/01/14 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 79% Analysis Date = 11/22/14 SpikeMix = NSI 032614: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 99% Analysis Date = 06/10/14 SpikeMix = Crescent 03DD004: 20 µl & NSI 032614: 20 µl Pct Recovery = 80% Analysis Date = 06/10/14 SpikeMix = NSI 032614: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 92% Analysis Date = 05/01/14 SpikeMix = Accu 214031115: 20 µl & NSI 032614: 20 µl Pct Recovery = 75% Analysis Date = 09/29/15 SpikeMix = Accu 215041380: 25 µl & ERA 0406-15-03: 25 µl Pct Recovery = 82% Analysis Date = 08/15/15 SpikeMix = Supelco LC13545: 25 µl & Crescent 04EE008: 25 µl Pct Recovery = 94% Analysis Date = 07/13/15 SpikeMix = Crescent 04EE008: 25 µl & NSI 050515AVOC: 25 µl Pct Recovery = 79% Analysis Date = 11/29/16 SpikeMix = ChemService 5082900: 15 µl & Phenova B20160319: 15 µl Pct Recovery = 89% Analysis Date = 09/08/16 SpikeMix = Phenova B20160319: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 81% Analysis Date = 07/29/16 SpikeMix = Phenova B20160319: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 88% Analysis Date = 05/27/16 SpikeMix = Phenova B20160319: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 95% Analysis Date = 10/13/16 SpikeMix = Accu 216041125: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 90% Analysis Date = 08/20/16 SpikeMix = Accu 216041125: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 85% Analysis Date = 06/30/16 SpikeMix = ChemService 5082900: 15 µl & Accu 216041125: 15 µl Pct Recovery = 68% Analysis Date = 04/02/16 SpikeMix = Supelco LC13545: 15 µl & Accu 215041380: 15 µl Pct Recovery = 89% Analysis Date = 03/04/16 SpikeMix = Accu 215041380: 15 µl & ERA 0406-15-03: 15 µl Pct Recovery = 84% Analysis Date = 06/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Accu 215041380: 15 µl Pct Recovery = 90% Analysis Date = 12/18/15 SpikeMix = Supelco LC13545: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 84% Analysis Date = 10/17/15 SpikeMix = Crescent 04EE008: 15 µl & NSI 050515AVOC: 15 µl Pct Recovery = 85% Analysis Date = 05/09/15 SpikeMix = Spex Organics EN150428007: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 96% Analysis Date = 01/13/15 SpikeMix = Accu 214031115: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 77% Analysis Date = 10/21/14 SpikeMix = ERA 0227-14-06.1A: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 86% Analysis Date = 10/04/14 SpikeMix = Crescent 03DD004: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 83% Analysis Date = 07/11/14 SpikeMix = Spex Organics C1140417015: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 92% Analysis Date = 09/09/14 SpikeMix = Accu 214031115: 10 µl & NSI 032614: 10 µl Pct Recovery = 107% Analysis Date = 09/09/14 SpikeMix = NSI 032614: 10 µl & Spex Organics C1140417015: 10 µl Pct Recovery = 104% Analysis Date = 07/29/14 SpikeMix = Crescent 03DD004: 10 µl & NSI 032614: 10 µl Pct Recovery = 96% Analysis Date = 05/30/14 SpikeMix = NSI 032614: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 73% Analysis Date = 02/18/16 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 89% Analysis Date = 11/20/15 SpikeMix = Accu 215041380: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 90% Analysis Date = 11/12/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 85% Analysis Date = 05/21/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 101% Analysis Date = 05/13/16 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 90% Analysis Date = 01/27/16 SpikeMix = Crescent 04EE008: 10 µl & NSI 050515AVOC: 10 µl Pct Recovery = 92% Analysis Date = 07/31/15 SpikeMix = Crescent 04EE008: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 80% Analysis Date = 05/09/15 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 89% Analysis Date = 12/11/16 Pct Recovery = 87% Analysis Date = 12/07/16 Pct Recovery = 87% Analysis Date = 12/07/16 Pct Recovery = 87% Analysis Date = 12/02/16 Pct Recovery = 87% Analysis Date = 12/02/16 Pct Recovery = 87% Analysis Date = 11/27/16 Pct Recovery = 87% Analysis Date = 11/27/16 Pct Recovery = 87% Analysis Date = 11/22/16 Pct Recovery = 87% Analysis Date = 11/22/16 Pct Recovery = 87% Analysis Date = 11/18/16 Pct Recovery = 87% Analysis Date = 11/18/16 Pct Recovery = 87% Analysis Date = 11/13/16 Pct Recovery = 87% Analysis Date = 11/13/16 Pct Recovery = 87% Analysis Date = 11/08/16 Pct Recovery = 87% Analysis Date = 11/08/16 Pct Recovery = 87% Analysis Date = 11/03/16 Pct Recovery = 87% Analysis Date = 11/03/16 Pct Recovery = 87% Analysis Date = 10/29/16 Pct Recovery = 87% Analysis Date = 10/29/16 Pct Recovery = 87% Analysis Date = 10/25/16 Pct Recovery = 87% Analysis Date = 10/25/16 Pct Recovery = 87% Analysis Date = 10/20/16 Pct Recovery = 87% Analysis Date = 10/20/16 Pct Recovery = 87% Analysis Date = 10/15/16 Pct Recovery = 87% Analysis Date = 10/15/16 Pct Recovery = 87% Analysis Date = 10/10/16 Pct Recovery = 87% Analysis Date = 10/10/16 Pct Recovery = 87% Analysis Date = 10/06/16 Pct Recovery = 87% Analysis Date = 10/06/16 Pct Recovery = 87% Analysis Date = 10/01/16 Pct Recovery = 87% Analysis Date = 10/01/16 Pct Recovery = 87% Analysis Date = 09/26/16 Pct Recovery = 87% Analysis Date = 09/26/16 Pct Recovery = 87% Analysis Date = 09/21/16 Pct Recovery = 87% Analysis Date = 09/21/16 Pct Recovery = 87% Analysis Date = 09/16/16 Pct Recovery = 87% Analysis Date = 09/16/16 Pct Recovery = 87% Analysis Date = 09/12/16 Pct Recovery = 87% Analysis Date = 09/12/16 Pct Recovery = 87% Analysis Date = 09/07/16 Pct Recovery = 87% Analysis Date = 09/07/16 Pct Recovery = 87% Analysis Date = 09/02/16 Pct Recovery = 87% Analysis Date = 09/02/16 Pct Recovery = 87% Analysis Date = 08/28/16 Pct Recovery = 87% Analysis Date = 08/28/16 Pct Recovery = 87% Analysis Date = 08/24/16 Pct Recovery = 87% Analysis Date = 08/24/16 Pct Recovery = 87% Analysis Date = 08/19/16 Pct Recovery = 87% Analysis Date = 08/19/16 Pct Recovery = 87% Analysis Date = 08/14/16 Pct Recovery = 87% Analysis Date = 08/14/16 Pct Recovery = 87% Analysis Date = 08/09/16 Pct Recovery = 87% Analysis Date = 08/09/16 Pct Recovery = 87% Analysis Date = 08/04/16 Pct Recovery = 87% Analysis Date = 08/04/16 Pct Recovery = 87% Analysis Date = 07/31/16 Pct Recovery = 87% Analysis Date = 07/31/16 Pct Recovery = 87% Analysis Date = 07/26/16 Pct Recovery = 87% Analysis Date = 07/26/16 Pct Recovery = 87% Analysis Date = 07/21/16 Pct Recovery = 87% Analysis Date = 07/21/16 Pct Recovery = 87% Analysis Date = 07/16/16 Pct Recovery = 87% Analysis Date = 07/16/16 Pct Recovery = 87% Analysis Date = 07/12/16 Pct Recovery = 87% Analysis Date = 07/12/16 Pct Recovery = 87% Analysis Date = 07/07/16 Pct Recovery = 87% Analysis Date = 07/07/16 Pct Recovery = 87% Analysis Date = 07/02/16 Pct Recovery = 87% Analysis Date = 07/02/16 Pct Recovery = 87% Analysis Date = 06/27/16 Pct Recovery = 87% Analysis Date = 06/27/16 Pct Recovery = 87% Analysis Date = 06/22/16 Pct Recovery = 87% Analysis Date = 06/22/16 Pct Recovery = 87% Analysis Date = 06/18/16 Pct Recovery = 87% Analysis Date = 06/18/16 Pct Recovery = 87% Analysis Date = 06/13/16 Pct Recovery = 87% Analysis Date = 06/13/16 Pct Recovery = 87% Analysis Date = 06/08/16 Pct Recovery = 87% Analysis Date = 06/08/16 Pct Recovery = 87% Analysis Date = 06/03/16 Pct Recovery = 87% Analysis Date = 06/03/16 Pct Recovery = 87% Analysis Date = 05/30/16 Pct Recovery = 87% Analysis Date = 05/30/16 Pct Recovery = 87% Analysis Date = 05/25/16 Pct Recovery = 87% Analysis Date = 05/25/16 Pct Recovery = 87% Analysis Date = 05/20/16 Pct Recovery = 87% Analysis Date = 05/20/16 Pct Recovery = 87% Analysis Date = 05/15/16 Pct Recovery = 87% Analysis Date = 05/15/16 Pct Recovery = 87% Analysis Date = 05/10/16 Pct Recovery = 87% Analysis Date = 05/10/16 Pct Recovery = 87% Analysis Date = 05/06/16 Pct Recovery = 87% Analysis Date = 05/06/16 Pct Recovery = 87% Analysis Date = 05/01/16 Pct Recovery = 87% Analysis Date = 05/01/16 Pct Recovery = 87% Analysis Date = 04/26/16 Pct Recovery = 87% Analysis Date = 04/26/16 Pct Recovery = 87% Analysis Date = 04/21/16 Pct Recovery = 87% Analysis Date = 04/21/16 Pct Recovery = 87% Analysis Date = 04/16/16 Pct Recovery = 87% Analysis Date = 04/16/16 Pct Recovery = 87% Analysis Date = 04/12/16 Pct Recovery = 87% Analysis Date = 04/12/16 Pct Recovery = 87% Analysis Date = 04/07/16 Pct Recovery = 87% Analysis Date = 04/07/16 Pct Recovery = 87% Analysis Date = 04/02/16 Pct Recovery = 87% Analysis Date = 04/02/16 Pct Recovery = 87% Analysis Date = 03/28/16 Pct Recovery = 87% Analysis Date = 03/28/16 Pct Recovery = 87% Analysis Date = 03/24/16 Pct Recovery = 87% Analysis Date = 03/24/16 Pct Recovery = 87% Analysis Date = 03/19/16 Pct Recovery = 87% Analysis Date = 03/19/16 Pct Recovery = 87% Analysis Date = 03/14/16 Pct Recovery = 87% Analysis Date = 03/14/16 Pct Recovery = 87% Analysis Date = 03/09/16 Pct Recovery = 87% Analysis Date = 03/09/16 Pct Recovery = 87% Analysis Date = 03/04/16 Pct Recovery = 87% Analysis Date = 03/04/16 Pct Recovery = 87% Analysis Date = 02/29/16 Pct Recovery = 87% Analysis Date = 02/29/16 Pct Recovery = 87% Analysis Date = 02/24/16 Pct Recovery = 87% Analysis Date = 02/24/16 Pct Recovery = 87% Analysis Date = 02/19/16 Pct Recovery = 87% Analysis Date = 02/19/16 Pct Recovery = 87% Analysis Date = 02/14/16 Pct Recovery = 87% Analysis Date = 02/14/16 Pct Recovery = 87% Analysis Date = 02/10/16 Pct Recovery = 87% Analysis Date = 02/10/16 Pct Recovery = 87% Analysis Date = 02/05/16 Pct Recovery = 87% Analysis Date = 02/05/16 Pct Recovery = 87% Analysis Date = 01/31/16 Pct Recovery = 87% Analysis Date = 01/31/16 Pct Recovery = 87% Analysis Date = 01/26/16 Pct Recovery = 87% Analysis Date = 01/26/16 Pct Recovery = 87% Analysis Date = 01/21/16 Pct Recovery = 87% Analysis Date = 01/21/16 Pct Recovery = 87% Analysis Date = 01/17/16 Pct Recovery = 87% Analysis Date = 01/17/16 Pct Recovery = 87% Analysis Date = 01/12/16 Pct Recovery = 87% Analysis Date = 01/12/16 Pct Recovery = 87% Analysis Date = 01/07/16 Pct Recovery = 87% Analysis Date = 01/07/16 Pct Recovery = 87% Analysis Date = 01/02/16 Pct Recovery = 87% Analysis Date = 01/02/16 Pct Recovery = 87% Analysis Date = 12/29/15 Pct Recovery = 87% Analysis Date = 12/29/15 Pct Recovery = 87% Analysis Date = 12/24/15 Pct Recovery = 87% Analysis Date = 12/24/15 Pct Recovery = 87% Analysis Date = 12/19/15 Pct Recovery = 87% Analysis Date = 12/19/15 Pct Recovery = 87% Analysis Date = 12/14/15 Pct Recovery = 87% Analysis Date = 12/14/15 Pct Recovery = 87% Analysis Date = 12/09/15 Pct Recovery = 87% Analysis Date = 12/09/15 Pct Recovery = 87% Analysis Date = 12/05/15 Pct Recovery = 87% Analysis Date = 12/05/15 Pct Recovery = 87% Analysis Date = 11/30/15 Pct Recovery = 87% Analysis Date = 11/30/15 Pct Recovery = 87% Analysis Date = 11/25/15 Pct Recovery = 87% Analysis Date = 11/25/15 Pct Recovery = 87% Analysis Date = 11/20/15 Pct Recovery = 87% Analysis Date = 11/20/15 Pct Recovery = 87% Analysis Date = 11/16/15 Pct Recovery = 87% Analysis Date = 11/16/15 Pct Recovery = 87% Analysis Date = 11/11/15 Pct Recovery = 87% Analysis Date = 11/11/15 Pct Recovery = 87% Analysis Date = 11/06/15 Pct Recovery = 87% Analysis Date = 11/06/15 Pct Recovery = 87% Analysis Date = 11/01/15 Pct Recovery = 87% Analysis Date = 11/01/15 Pct Recovery = 87% Analysis Date = 10/27/15 Pct Recovery = 87% Analysis Date = 10/27/15 Pct Recovery = 87% Analysis Date = 10/23/15 Pct Recovery = 87% Analysis Date = 10/23/15 Pct Recovery = 87% Analysis Date = 10/18/15 Pct Recovery = 87% Analysis Date = 10/18/15 Pct Recovery = 87% Analysis Date = 10/13/15 Pct Recovery = 87% Analysis Date = 10/13/15 Pct Recovery = 87% Analysis Date = 10/08/15 Pct Recovery = 87% Analysis Date = 10/08/15 Pct Recovery = 87% Analysis Date = 10/04/15 Pct Recovery = 87% Analysis Date = 10/04/15 Pct Recovery = 87% Analysis Date = 09/29/15 Pct Recovery = 87% Analysis Date = 09/29/15 Pct Recovery = 87% Analysis Date = 09/24/15 Pct Recovery = 87% Analysis Date = 09/24/15 Pct Recovery = 87% Analysis Date = 09/19/15 Pct Recovery = 88% Analysis Date = 09/19/15 Pct Recovery = 88% Analysis Date = 09/14/15 Pct Recovery = 88% Analysis Date = 09/14/15 Pct Recovery = 88% Analysis Date = 09/10/15 Pct Recovery = 88% Analysis Date = 09/10/15 Pct Recovery = 88% Analysis Date = 09/05/15 Pct Recovery = 88% Analysis Date = 09/05/15 Pct Recovery = 88% Analysis Date = 08/31/15 Pct Recovery = 88% Analysis Date = 08/31/15 Pct Recovery = 88% Analysis Date = 08/26/15 Pct Recovery = 88% Analysis Date = 08/26/15 Pct Recovery = 88% Analysis Date = 08/21/15 Pct Recovery = 88% Analysis Date = 08/21/15 Pct Recovery = 88% Analysis Date = 08/17/15 Pct Recovery = 88% Analysis Date = 08/17/15 Pct Recovery = 88% Analysis Date = 08/12/15 Pct Recovery = 88% Analysis Date = 08/12/15 Pct Recovery = 88% Analysis Date = 08/07/15 Pct Recovery = 88% Analysis Date = 08/07/15 Pct Recovery = 88% Analysis Date = 08/02/15 Pct Recovery = 88% Analysis Date = 08/02/15 Pct Recovery = 88% Analysis Date = 07/29/15 Pct Recovery = 88% Analysis Date = 07/29/15 Pct Recovery = 88% Analysis Date = 07/24/15 Pct Recovery = 88% Analysis Date = 07/24/15 Pct Recovery = 88% Analysis Date = 07/19/15 Pct Recovery = 88% Analysis Date = 07/19/15 Pct Recovery = 88% Analysis Date = 07/14/15 Pct Recovery = 88% Analysis Date = 07/14/15 Pct Recovery = 88% Analysis Date = 07/09/15 Pct Recovery = 88% Analysis Date = 07/09/15 Pct Recovery = 88% Analysis Date = 07/05/15 Pct Recovery = 88% Analysis Date = 07/05/15 Pct Recovery = 88% Analysis Date = 06/30/15 Pct Recovery = 88% Analysis Date = 06/30/15 Pct Recovery = 88% Analysis Date = 06/25/15 Pct Recovery = 88% Analysis Date = 06/25/15 Pct Recovery = 88% Analysis Date = 06/20/15 Pct Recovery = 88% Analysis Date = 06/20/15 Pct Recovery = 88% Analysis Date = 06/16/15 Pct Recovery = 88% Analysis Date = 06/16/15 Pct Recovery = 88% Analysis Date = 06/11/15 Pct Recovery = 88% Analysis Date = 06/11/15 Pct Recovery = 88% Analysis Date = 06/06/15 Pct Recovery = 88% Analysis Date = 06/06/15 Pct Recovery = 88% Analysis Date = 06/01/15 Pct Recovery = 88% Analysis Date = 06/01/15 Pct Recovery = 88% Analysis Date = 05/27/15 Pct Recovery = 88% Analysis Date = 05/27/15 Pct Recovery = 88% Analysis Date = 05/23/15 Pct Recovery = 88% Analysis Date = 05/23/15 Pct Recovery = 88% Analysis Date = 05/18/15 Pct Recovery = 88% Analysis Date = 05/18/15 Pct Recovery = 88% Analysis Date = 05/13/15 Pct Recovery = 88% Analysis Date = 05/13/15 Pct Recovery = 88% Analysis Date = 05/08/15 Pct Recovery = 88% Analysis Date = 05/08/15 Pct Recovery = 88% Analysis Date = 05/04/15 Pct Recovery = 88% Analysis Date = 05/04/15 Pct Recovery = 88% Analysis Date = 04/29/15 Pct Recovery = 88% Analysis Date = 04/29/15 Pct Recovery = 88% Analysis Date = 04/24/15 Pct Recovery = 88% Analysis Date = 04/24/15 Pct Recovery = 88% Analysis Date = 04/19/15 Pct Recovery = 88% Analysis Date = 04/19/15 Pct Recovery = 88% Analysis Date = 04/14/15 Pct Recovery = 88% Analysis Date = 04/14/15 Pct Recovery = 88% Analysis Date = 04/10/15 Pct Recovery = 88% Analysis Date = 04/10/15 Pct Recovery = 88% Analysis Date = 04/05/15 Pct Recovery = 88% Analysis Date = 04/05/15 Pct Recovery = 88% Analysis Date = 03/31/15 Pct Recovery = 89% Analysis Date = 03/31/15 Pct Recovery = 89% Analysis Date = 03/26/15 Pct Recovery = 89% Analysis Date = 03/26/15 Pct Recovery = 89% Analysis Date = 03/22/15 Pct Recovery = 89% Analysis Date = 03/22/15 Pct Recovery = 89% Analysis Date = 03/17/15 Pct Recovery = 89% Analysis Date = 03/17/15 Pct Recovery = 89% Analysis Date = 03/12/15 Pct Recovery = 89% Analysis Date = 03/12/15 Pct Recovery = 89% Analysis Date = 03/07/15 Pct Recovery = 89% Analysis Date = 03/07/15 Pct Recovery = 89% Analysis Date = 03/02/15 Pct Recovery = 89% Analysis Date = 03/02/15 Pct Recovery = 89% Analysis Date = 02/26/15 Pct Recovery = 89% Analysis Date = 02/26/15 Pct Recovery = 89% Analysis Date = 02/21/15 Pct Recovery = 89% Analysis Date = 02/21/15 Pct Recovery = 89% Analysis Date = 02/16/15 Pct Recovery = 89% Analysis Date = 02/16/15 Pct Recovery = 89% Analysis Date = 02/11/15 Pct Recovery = 89% Analysis Date = 02/11/15 Pct Recovery = 89% Analysis Date = 02/07/15 Pct Recovery = 89% Analysis Date = 02/07/15 Pct Recovery = 89% Analysis Date = 02/02/15 Pct Recovery = 89% Analysis Date = 02/02/15 Pct Recovery = 89% Analysis Date = 01/28/15 Pct Recovery = 89% Analysis Date = 01/28/15 Pct Recovery = 89% Analysis Date = 01/23/15 Pct Recovery = 89% Analysis Date = 01/23/15 Pct Recovery = 89% Analysis Date = 01/18/15 Pct Recovery = 89% Analysis Date = 01/18/15 Pct Recovery = 89% Analysis Date = 01/14/15 Pct Recovery = 89% Analysis Date = 01/14/15 Pct Recovery = 89% Analysis Date = 01/09/15 Pct Recovery = 89% Analysis Date = 01/09/15 Pct Recovery = 89% Analysis Date = 01/04/15 Pct Recovery = 89% Analysis Date = 01/04/15 Pct Recovery = 89% Analysis Date = 12/30/14 Pct Recovery = 89% Analysis Date = 12/30/14 Pct Recovery = 89% Analysis Date = 12/25/14 Pct Recovery = 89% Analysis Date = 12/25/14 Pct Recovery = 89% Analysis Date = 12/21/14 Pct Recovery = 89% Analysis Date = 12/21/14 Pct Recovery = 89% Analysis Date = 12/16/14 Pct Recovery = 89% Analysis Date = 12/16/14 Pct Recovery = 89% Analysis Date = 12/11/14 Pct Recovery = 89% Analysis Date = 12/11/14 Pct Recovery = 89% Analysis Date = 12/06/14 Pct Recovery = 89% Analysis Date = 12/06/14 Pct Recovery = 89% Analysis Date = 12/02/14 Pct Recovery = 89% Analysis Date = 12/02/14 Pct Recovery = 89% Analysis Date = 11/27/14 Pct Recovery = 89% Analysis Date = 11/27/14 Pct Recovery = 89% Analysis Date = 11/22/14 Pct Recovery = 89% Analysis Date = 11/22/14 Pct Recovery = 89% Analysis Date = 11/17/14 Pct Recovery = 89% Analysis Date = 11/17/14 Pct Recovery = 89% Analysis Date = 11/12/14 Pct Recovery = 89% Analysis Date = 11/12/14 Pct Recovery = 89% Analysis Date = 11/08/14 Pct Recovery = 88% Analysis Date = 11/08/14 Pct Recovery = 88% Analysis Date = 11/03/14 Pct Recovery = 88% Analysis Date = 11/03/14 Pct Recovery = 88% Analysis Date = 10/29/14 Pct Recovery = 88% Analysis Date = 10/29/14 Pct Recovery = 88% Analysis Date = 10/24/14 Pct Recovery = 88% Analysis Date = 10/24/14 Pct Recovery = 88% Analysis Date = 10/20/14 Pct Recovery = 88% Analysis Date = 10/20/14 Pct Recovery = 88% Analysis Date = 10/15/14 Pct Recovery = 88% Analysis Date = 10/15/14 Pct Recovery = 88% Analysis Date = 10/10/14 Pct Recovery = 88% Analysis Date = 10/10/14 Pct Recovery = 88% Analysis Date = 10/05/14 Pct Recovery = 88% Analysis Date = 10/05/14 Pct Recovery = 88% Analysis Date = 09/30/14 Pct Recovery = 88% Analysis Date = 09/30/14 Pct Recovery = 88% Analysis Date = 09/26/14 Pct Recovery = 88% Analysis Date = 09/26/14 Pct Recovery = 88% Analysis Date = 09/21/14 Pct Recovery = 88% Analysis Date = 09/21/14 Pct Recovery = 88% Analysis Date = 09/16/14 Pct Recovery = 88% Analysis Date = 09/16/14 Pct Recovery = 88% Analysis Date = 09/11/14 Pct Recovery = 88% Analysis Date = 09/11/14 Pct Recovery = 88% Analysis Date = 09/07/14 Pct Recovery = 88% Analysis Date = 09/07/14 Pct Recovery = 88% Analysis Date = 09/02/14 Pct Recovery = 87% Analysis Date = 09/02/14 Pct Recovery = 87% Analysis Date = 08/28/14 Pct Recovery = 87% Analysis Date = 08/28/14 Pct Recovery = 87% Analysis Date = 08/23/14 Pct Recovery = 87% Analysis Date = 08/23/14 Pct Recovery = 87% Analysis Date = 08/18/14 Pct Recovery = 87% Analysis Date = 08/18/14 Pct Recovery = 87% Analysis Date = 08/14/14 Pct Recovery = 87% Analysis Date = 08/14/14 Pct Recovery = 87% Analysis Date = 08/09/14 Pct Recovery = 87% Analysis Date = 08/09/14 Pct Recovery = 87% Analysis Date = 08/04/14 Pct Recovery = 87% Analysis Date = 08/04/14 Pct Recovery = 87% Analysis Date = 07/30/14 Pct Recovery = 87% Analysis Date = 07/30/14 Pct Recovery = 87% Analysis Date = 07/26/14 Pct Recovery = 87% Analysis Date = 07/26/14 Pct Recovery = 87% Analysis Date = 07/21/14 Pct Recovery = 87% Analysis Date = 07/21/14 Pct Recovery = 87% Analysis Date = 07/16/14 Pct Recovery = 87% Analysis Date = 07/16/14 Pct Recovery = 87% Analysis Date = 07/11/14 Pct Recovery = 87% Analysis Date = 07/11/14 Pct Recovery = 87% Analysis Date = 07/06/14 Pct Recovery = 87% Analysis Date = 07/06/14 Pct Recovery = 87% Analysis Date = 07/02/14 Pct Recovery = 86% Analysis Date = 07/02/14 Pct Recovery = 86% Analysis Date = 06/27/14 Pct Recovery = 86% Analysis Date = 06/27/14 Pct Recovery = 86% Analysis Date = 06/22/14 Pct Recovery = 86% Analysis Date = 06/22/14 Pct Recovery = 86% Analysis Date = 06/17/14 Pct Recovery = 86% Analysis Date = 06/17/14 Pct Recovery = 86% Analysis Date = 06/13/14 Pct Recovery = 86% Analysis Date = 06/13/14 Pct Recovery = 86% Analysis Date = 06/08/14 Pct Recovery = 86% Analysis Date = 06/08/14 Pct Recovery = 86% Analysis Date = 06/03/14 Pct Recovery = 86% Analysis Date = 06/03/14 Pct Recovery = 86% Analysis Date = 05/29/14 Pct Recovery = 86% Analysis Date = 05/29/14 Pct Recovery = 86% Analysis Date = 05/24/14 Pct Recovery = 86% Analysis Date = 05/24/14 Pct Recovery = 86% Analysis Date = 05/20/14 Pct Recovery = 86% Analysis Date = 05/20/14 Pct Recovery = 86% Analysis Date = 05/15/14 Pct Recovery = 86% Analysis Date = 05/15/14 Pct Recovery = 86% Analysis Date = 05/10/14 Pct Recovery = 85% Analysis Date = 05/10/14 Pct Recovery = 85% Analysis Date = 05/05/14 Pct Recovery = 85% Analysis Date = 05/05/14 Pct Recovery = 85% Analysis Date = 05/01/14 Pct Recovery = 85% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
4-CHLOROTOLUENE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 48 87% 8% 87% 8%
Total 48 87% 8% 87% 8%

Sample Statistics
4-CHLOROTOLUENE

Characteristic N % % Basis
Plotted 48 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 48 .  
False Negatives 0 0% 0 out of 48
Not Spiked 25 .  
False Positives 0 0% 0 out of 25

BQS OBSP Determination:
4-ISOPROPYL-1-METHYLBENZENE (CYMENE)
METHOD: 4440 , TESTIDCODE: 77356GCM66
Open Data Set

Analysis Date = 12/12/16 SpikeMix = Accu 216041125: 40 µl & Crescent 03FF058: 40 µl Pct Recovery = 91% Analysis Date = 07/20/16 SpikeMix = Supelco LC20141V: 40 µl & Accu 216041125: 40 µl Pct Recovery = 79% Analysis Date = 07/14/16 SpikeMix = Accu 216041125: 40 µl & NSI 041816AVOC: 40 µl Pct Recovery = 74% Analysis Date = 08/12/16 SpikeMix = ChemService 5082900: 25 µl & Phenova B20160319: 25 µl Pct Recovery = 71% Analysis Date = 06/21/16 SpikeMix = Phenova B20160319: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 89% Analysis Date = 09/08/16 SpikeMix = Supelco LC20141V: 25 µl & Accu 216041125: 25 µl Pct Recovery = 60% Analysis Date = 05/24/16 SpikeMix = Accu 216041125: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 79% Analysis Date = 04/09/15 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 74% Analysis Date = 03/06/15 SpikeMix = ERA 0227-14-06.1A: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 78% Analysis Date = 11/14/14 SpikeMix = Crescent 03DD004: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 69% Analysis Date = 08/16/14 SpikeMix = ERA 0227-14-06.1A: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 78% Analysis Date = 07/01/14 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 71% Analysis Date = 11/22/14 SpikeMix = NSI 032614: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 76% Analysis Date = 06/10/14 SpikeMix = Crescent 03DD004: 20 µl & NSI 032614: 20 µl Pct Recovery = 67% Analysis Date = 06/10/14 SpikeMix = NSI 032614: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 76% Analysis Date = 05/01/14 SpikeMix = Accu 214031115: 20 µl & NSI 032614: 20 µl Pct Recovery = 62% Analysis Date = 08/15/15 SpikeMix = Supelco LC13545: 25 µl & Crescent 04EE008: 25 µl Pct Recovery = 91% Analysis Date = 06/16/15 SpikeMix = ERA 0406-15-03: 25 µl & Supelco LC13545: 25 µl Pct Recovery = 78% Analysis Date = 11/29/16 SpikeMix = ChemService 5082900: 15 µl & Phenova B20160319: 15 µl Pct Recovery = 74% Analysis Date = 09/08/16 SpikeMix = Phenova B20160319: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 77% Analysis Date = 07/29/16 SpikeMix = Phenova B20160319: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 85% Analysis Date = 05/27/16 SpikeMix = Phenova B20160319: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 79% Analysis Date = 10/13/16 SpikeMix = Accu 216041125: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 72% Analysis Date = 08/20/16 SpikeMix = Accu 216041125: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 75% Analysis Date = 06/30/16 SpikeMix = ChemService 5082900: 15 µl & Accu 216041125: 15 µl Pct Recovery = 50% Analysis Date = 04/26/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 74% Analysis Date = 02/05/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 83% Analysis Date = 11/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 90% Analysis Date = 10/16/15 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 82% Analysis Date = 05/09/15 SpikeMix = Spex Organics EN150428007: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 84% Analysis Date = 04/02/16 SpikeMix = Supelco LC13545: 15 µl & Accu 215041380: 15 µl Pct Recovery = 79% Analysis Date = 12/18/15 SpikeMix = Supelco LC13545: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 82% Analysis Date = 01/13/15 SpikeMix = Accu 214031115: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 75% Analysis Date = 10/21/14 SpikeMix = ERA 0227-14-06.1A: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 78% Analysis Date = 10/04/14 SpikeMix = Crescent 03DD004: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 80% Analysis Date = 07/11/14 SpikeMix = Spex Organics C1140417015: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 81% Analysis Date = 09/09/14 SpikeMix = Accu 214031115: 10 µl & NSI 032614: 10 µl Pct Recovery = 97% Analysis Date = 09/09/14 SpikeMix = NSI 032614: 10 µl & Spex Organics C1140417015: 10 µl Pct Recovery = 96% Analysis Date = 07/29/14 SpikeMix = Crescent 03DD004: 10 µl & NSI 032614: 10 µl Pct Recovery = 79% Analysis Date = 05/30/14 SpikeMix = NSI 032614: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 60% Analysis Date = 02/18/16 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 85% Analysis Date = 11/12/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 106% Analysis Date = 09/03/15 SpikeMix = NSI 050515AVOC: 10 µl & Spex Organics EN150428007: 10 µl Pct Recovery = 75% Analysis Date = 05/21/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 89% Analysis Date = 05/13/16 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 83% Analysis Date = 03/17/16 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 67% Analysis Date = 12/10/15 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 82% Analysis Date = 06/27/15 SpikeMix = ERA 0406-15-03: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 88% Analysis Date = 05/09/15 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 83% Analysis Date = 12/11/16 Pct Recovery = 73% Analysis Date = 12/07/16 Pct Recovery = 73% Analysis Date = 12/07/16 Pct Recovery = 73% Analysis Date = 12/02/16 Pct Recovery = 73% Analysis Date = 12/02/16 Pct Recovery = 73% Analysis Date = 11/27/16 Pct Recovery = 73% Analysis Date = 11/27/16 Pct Recovery = 73% Analysis Date = 11/22/16 Pct Recovery = 74% Analysis Date = 11/22/16 Pct Recovery = 74% Analysis Date = 11/18/16 Pct Recovery = 74% Analysis Date = 11/18/16 Pct Recovery = 74% Analysis Date = 11/13/16 Pct Recovery = 74% Analysis Date = 11/13/16 Pct Recovery = 74% Analysis Date = 11/08/16 Pct Recovery = 74% Analysis Date = 11/08/16 Pct Recovery = 74% Analysis Date = 11/03/16 Pct Recovery = 74% Analysis Date = 11/03/16 Pct Recovery = 74% Analysis Date = 10/29/16 Pct Recovery = 74% Analysis Date = 10/29/16 Pct Recovery = 74% Analysis Date = 10/25/16 Pct Recovery = 74% Analysis Date = 10/25/16 Pct Recovery = 74% Analysis Date = 10/20/16 Pct Recovery = 74% Analysis Date = 10/20/16 Pct Recovery = 74% Analysis Date = 10/15/16 Pct Recovery = 74% Analysis Date = 10/15/16 Pct Recovery = 74% Analysis Date = 10/10/16 Pct Recovery = 74% Analysis Date = 10/10/16 Pct Recovery = 74% Analysis Date = 10/06/16 Pct Recovery = 74% Analysis Date = 10/06/16 Pct Recovery = 74% Analysis Date = 10/01/16 Pct Recovery = 75% Analysis Date = 10/01/16 Pct Recovery = 75% Analysis Date = 09/26/16 Pct Recovery = 75% Analysis Date = 09/26/16 Pct Recovery = 75% Analysis Date = 09/21/16 Pct Recovery = 75% Analysis Date = 09/21/16 Pct Recovery = 75% Analysis Date = 09/16/16 Pct Recovery = 75% Analysis Date = 09/16/16 Pct Recovery = 75% Analysis Date = 09/12/16 Pct Recovery = 75% Analysis Date = 09/12/16 Pct Recovery = 75% Analysis Date = 09/07/16 Pct Recovery = 75% Analysis Date = 09/07/16 Pct Recovery = 75% Analysis Date = 09/02/16 Pct Recovery = 75% Analysis Date = 09/02/16 Pct Recovery = 75% Analysis Date = 08/28/16 Pct Recovery = 75% Analysis Date = 08/28/16 Pct Recovery = 75% Analysis Date = 08/24/16 Pct Recovery = 75% Analysis Date = 08/24/16 Pct Recovery = 75% Analysis Date = 08/19/16 Pct Recovery = 76% Analysis Date = 08/19/16 Pct Recovery = 76% Analysis Date = 08/14/16 Pct Recovery = 76% Analysis Date = 08/14/16 Pct Recovery = 76% Analysis Date = 08/09/16 Pct Recovery = 76% Analysis Date = 08/09/16 Pct Recovery = 76% Analysis Date = 08/04/16 Pct Recovery = 76% Analysis Date = 08/04/16 Pct Recovery = 76% Analysis Date = 07/31/16 Pct Recovery = 76% Analysis Date = 07/31/16 Pct Recovery = 76% Analysis Date = 07/26/16 Pct Recovery = 76% Analysis Date = 07/26/16 Pct Recovery = 76% Analysis Date = 07/21/16 Pct Recovery = 76% Analysis Date = 07/21/16 Pct Recovery = 76% Analysis Date = 07/16/16 Pct Recovery = 76% Analysis Date = 07/16/16 Pct Recovery = 76% Analysis Date = 07/12/16 Pct Recovery = 76% Analysis Date = 07/12/16 Pct Recovery = 76% Analysis Date = 07/07/16 Pct Recovery = 77% Analysis Date = 07/07/16 Pct Recovery = 77% Analysis Date = 07/02/16 Pct Recovery = 77% Analysis Date = 07/02/16 Pct Recovery = 77% Analysis Date = 06/27/16 Pct Recovery = 77% Analysis Date = 06/27/16 Pct Recovery = 77% Analysis Date = 06/22/16 Pct Recovery = 77% Analysis Date = 06/22/16 Pct Recovery = 77% Analysis Date = 06/18/16 Pct Recovery = 77% Analysis Date = 06/18/16 Pct Recovery = 77% Analysis Date = 06/13/16 Pct Recovery = 77% Analysis Date = 06/13/16 Pct Recovery = 77% Analysis Date = 06/08/16 Pct Recovery = 77% Analysis Date = 06/08/16 Pct Recovery = 77% Analysis Date = 06/03/16 Pct Recovery = 77% Analysis Date = 06/03/16 Pct Recovery = 77% Analysis Date = 05/30/16 Pct Recovery = 78% Analysis Date = 05/30/16 Pct Recovery = 78% Analysis Date = 05/25/16 Pct Recovery = 78% Analysis Date = 05/25/16 Pct Recovery = 78% Analysis Date = 05/20/16 Pct Recovery = 78% Analysis Date = 05/20/16 Pct Recovery = 78% Analysis Date = 05/15/16 Pct Recovery = 78% Analysis Date = 05/15/16 Pct Recovery = 78% Analysis Date = 05/10/16 Pct Recovery = 78% Analysis Date = 05/10/16 Pct Recovery = 78% Analysis Date = 05/06/16 Pct Recovery = 78% Analysis Date = 05/06/16 Pct Recovery = 78% Analysis Date = 05/01/16 Pct Recovery = 79% Analysis Date = 05/01/16 Pct Recovery = 79% Analysis Date = 04/26/16 Pct Recovery = 79% Analysis Date = 04/26/16 Pct Recovery = 79% Analysis Date = 04/21/16 Pct Recovery = 79% Analysis Date = 04/21/16 Pct Recovery = 79% Analysis Date = 04/16/16 Pct Recovery = 79% Analysis Date = 04/16/16 Pct Recovery = 79% Analysis Date = 04/12/16 Pct Recovery = 79% Analysis Date = 04/12/16 Pct Recovery = 79% Analysis Date = 04/07/16 Pct Recovery = 79% Analysis Date = 04/07/16 Pct Recovery = 79% Analysis Date = 04/02/16 Pct Recovery = 80% Analysis Date = 04/02/16 Pct Recovery = 80% Analysis Date = 03/28/16 Pct Recovery = 80% Analysis Date = 03/28/16 Pct Recovery = 80% Analysis Date = 03/24/16 Pct Recovery = 80% Analysis Date = 03/24/16 Pct Recovery = 80% Analysis Date = 03/19/16 Pct Recovery = 80% Analysis Date = 03/19/16 Pct Recovery = 80% Analysis Date = 03/14/16 Pct Recovery = 80% Analysis Date = 03/14/16 Pct Recovery = 80% Analysis Date = 03/09/16 Pct Recovery = 81% Analysis Date = 03/09/16 Pct Recovery = 81% Analysis Date = 03/04/16 Pct Recovery = 81% Analysis Date = 03/04/16 Pct Recovery = 81% Analysis Date = 02/29/16 Pct Recovery = 81% Analysis Date = 02/29/16 Pct Recovery = 81% Analysis Date = 02/24/16 Pct Recovery = 81% Analysis Date = 02/24/16 Pct Recovery = 81% Analysis Date = 02/19/16 Pct Recovery = 81% Analysis Date = 02/19/16 Pct Recovery = 81% Analysis Date = 02/14/16 Pct Recovery = 82% Analysis Date = 02/14/16 Pct Recovery = 82% Analysis Date = 02/10/16 Pct Recovery = 82% Analysis Date = 02/10/16 Pct Recovery = 82% Analysis Date = 02/05/16 Pct Recovery = 82% Analysis Date = 02/05/16 Pct Recovery = 82% Analysis Date = 01/31/16 Pct Recovery = 82% Analysis Date = 01/31/16 Pct Recovery = 82% Analysis Date = 01/26/16 Pct Recovery = 82% Analysis Date = 01/26/16 Pct Recovery = 82% Analysis Date = 01/21/16 Pct Recovery = 82% Analysis Date = 01/21/16 Pct Recovery = 82% Analysis Date = 01/17/16 Pct Recovery = 82% Analysis Date = 01/17/16 Pct Recovery = 82% Analysis Date = 01/12/16 Pct Recovery = 83% Analysis Date = 01/12/16 Pct Recovery = 83% Analysis Date = 01/07/16 Pct Recovery = 83% Analysis Date = 01/07/16 Pct Recovery = 83% Analysis Date = 01/02/16 Pct Recovery = 83% Analysis Date = 01/02/16 Pct Recovery = 83% Analysis Date = 12/29/15 Pct Recovery = 83% Analysis Date = 12/29/15 Pct Recovery = 83% Analysis Date = 12/24/15 Pct Recovery = 83% Analysis Date = 12/24/15 Pct Recovery = 83% Analysis Date = 12/19/15 Pct Recovery = 83% Analysis Date = 12/19/15 Pct Recovery = 83% Analysis Date = 12/14/15 Pct Recovery = 83% Analysis Date = 12/14/15 Pct Recovery = 83% Analysis Date = 12/09/15 Pct Recovery = 83% Analysis Date = 12/09/15 Pct Recovery = 83% Analysis Date = 12/05/15 Pct Recovery = 83% Analysis Date = 12/05/15 Pct Recovery = 83% Analysis Date = 11/30/15 Pct Recovery = 84% Analysis Date = 11/30/15 Pct Recovery = 84% Analysis Date = 11/25/15 Pct Recovery = 84% Analysis Date = 11/25/15 Pct Recovery = 84% Analysis Date = 11/20/15 Pct Recovery = 84% Analysis Date = 11/20/15 Pct Recovery = 84% Analysis Date = 11/16/15 Pct Recovery = 84% Analysis Date = 11/16/15 Pct Recovery = 84% Analysis Date = 11/11/15 Pct Recovery = 84% Analysis Date = 11/11/15 Pct Recovery = 84% Analysis Date = 11/06/15 Pct Recovery = 84% Analysis Date = 11/06/15 Pct Recovery = 84% Analysis Date = 11/01/15 Pct Recovery = 84% Analysis Date = 11/01/15 Pct Recovery = 84% Analysis Date = 10/27/15 Pct Recovery = 84% Analysis Date = 10/27/15 Pct Recovery = 84% Analysis Date = 10/23/15 Pct Recovery = 84% Analysis Date = 10/23/15 Pct Recovery = 84% Analysis Date = 10/18/15 Pct Recovery = 84% Analysis Date = 10/18/15 Pct Recovery = 84% Analysis Date = 10/13/15 Pct Recovery = 84% Analysis Date = 10/13/15 Pct Recovery = 84% Analysis Date = 10/08/15 Pct Recovery = 84% Analysis Date = 10/08/15 Pct Recovery = 84% Analysis Date = 10/04/15 Pct Recovery = 84% Analysis Date = 10/04/15 Pct Recovery = 84% Analysis Date = 09/29/15 Pct Recovery = 84% Analysis Date = 09/29/15 Pct Recovery = 84% Analysis Date = 09/24/15 Pct Recovery = 84% Analysis Date = 09/24/15 Pct Recovery = 84% Analysis Date = 09/19/15 Pct Recovery = 84% Analysis Date = 09/19/15 Pct Recovery = 84% Analysis Date = 09/14/15 Pct Recovery = 84% Analysis Date = 09/14/15 Pct Recovery = 84% Analysis Date = 09/10/15 Pct Recovery = 84% Analysis Date = 09/10/15 Pct Recovery = 84% Analysis Date = 09/05/15 Pct Recovery = 83% Analysis Date = 09/05/15 Pct Recovery = 83% Analysis Date = 08/31/15 Pct Recovery = 83% Analysis Date = 08/31/15 Pct Recovery = 83% Analysis Date = 08/26/15 Pct Recovery = 83% Analysis Date = 08/26/15 Pct Recovery = 83% Analysis Date = 08/21/15 Pct Recovery = 83% Analysis Date = 08/21/15 Pct Recovery = 83% Analysis Date = 08/17/15 Pct Recovery = 83% Analysis Date = 08/17/15 Pct Recovery = 83% Analysis Date = 08/12/15 Pct Recovery = 83% Analysis Date = 08/12/15 Pct Recovery = 83% Analysis Date = 08/07/15 Pct Recovery = 83% Analysis Date = 08/07/15 Pct Recovery = 83% Analysis Date = 08/02/15 Pct Recovery = 83% Analysis Date = 08/02/15 Pct Recovery = 83% Analysis Date = 07/29/15 Pct Recovery = 83% Analysis Date = 07/29/15 Pct Recovery = 83% Analysis Date = 07/24/15 Pct Recovery = 83% Analysis Date = 07/24/15 Pct Recovery = 83% Analysis Date = 07/19/15 Pct Recovery = 83% Analysis Date = 07/19/15 Pct Recovery = 83% Analysis Date = 07/14/15 Pct Recovery = 83% Analysis Date = 07/14/15 Pct Recovery = 83% Analysis Date = 07/09/15 Pct Recovery = 83% Analysis Date = 07/09/15 Pct Recovery = 83% Analysis Date = 07/05/15 Pct Recovery = 83% Analysis Date = 07/05/15 Pct Recovery = 83% Analysis Date = 06/30/15 Pct Recovery = 83% Analysis Date = 06/30/15 Pct Recovery = 83% Analysis Date = 06/25/15 Pct Recovery = 83% Analysis Date = 06/25/15 Pct Recovery = 83% Analysis Date = 06/20/15 Pct Recovery = 83% Analysis Date = 06/20/15 Pct Recovery = 83% Analysis Date = 06/16/15 Pct Recovery = 83% Analysis Date = 06/16/15 Pct Recovery = 83% Analysis Date = 06/11/15 Pct Recovery = 83% Analysis Date = 06/11/15 Pct Recovery = 83% Analysis Date = 06/06/15 Pct Recovery = 83% Analysis Date = 06/06/15 Pct Recovery = 83% Analysis Date = 06/01/15 Pct Recovery = 83% Analysis Date = 06/01/15 Pct Recovery = 83% Analysis Date = 05/27/15 Pct Recovery = 83% Analysis Date = 05/27/15 Pct Recovery = 83% Analysis Date = 05/23/15 Pct Recovery = 82% Analysis Date = 05/23/15 Pct Recovery = 82% Analysis Date = 05/18/15 Pct Recovery = 82% Analysis Date = 05/18/15 Pct Recovery = 82% Analysis Date = 05/13/15 Pct Recovery = 82% Analysis Date = 05/13/15 Pct Recovery = 82% Analysis Date = 05/08/15 Pct Recovery = 82% Analysis Date = 05/08/15 Pct Recovery = 82% Analysis Date = 05/04/15 Pct Recovery = 82% Analysis Date = 05/04/15 Pct Recovery = 82% Analysis Date = 04/29/15 Pct Recovery = 82% Analysis Date = 04/29/15 Pct Recovery = 82% Analysis Date = 04/24/15 Pct Recovery = 82% Analysis Date = 04/24/15 Pct Recovery = 82% Analysis Date = 04/19/15 Pct Recovery = 82% Analysis Date = 04/19/15 Pct Recovery = 82% Analysis Date = 04/14/15 Pct Recovery = 82% Analysis Date = 04/14/15 Pct Recovery = 82% Analysis Date = 04/10/15 Pct Recovery = 82% Analysis Date = 04/10/15 Pct Recovery = 82% Analysis Date = 04/05/15 Pct Recovery = 82% Analysis Date = 04/05/15 Pct Recovery = 82% Analysis Date = 03/31/15 Pct Recovery = 82% Analysis Date = 03/31/15 Pct Recovery = 82% Analysis Date = 03/26/15 Pct Recovery = 82% Analysis Date = 03/26/15 Pct Recovery = 82% Analysis Date = 03/22/15 Pct Recovery = 82% Analysis Date = 03/22/15 Pct Recovery = 82% Analysis Date = 03/17/15 Pct Recovery = 81% Analysis Date = 03/17/15 Pct Recovery = 81% Analysis Date = 03/12/15 Pct Recovery = 81% Analysis Date = 03/12/15 Pct Recovery = 81% Analysis Date = 03/07/15 Pct Recovery = 81% Analysis Date = 03/07/15 Pct Recovery = 81% Analysis Date = 03/02/15 Pct Recovery = 81% Analysis Date = 03/02/15 Pct Recovery = 81% Analysis Date = 02/26/15 Pct Recovery = 81% Analysis Date = 02/26/15 Pct Recovery = 81% Analysis Date = 02/21/15 Pct Recovery = 81% Analysis Date = 02/21/15 Pct Recovery = 81% Analysis Date = 02/16/15 Pct Recovery = 81% Analysis Date = 02/16/15 Pct Recovery = 81% Analysis Date = 02/11/15 Pct Recovery = 81% Analysis Date = 02/11/15 Pct Recovery = 81% Analysis Date = 02/07/15 Pct Recovery = 81% Analysis Date = 02/07/15 Pct Recovery = 81% Analysis Date = 02/02/15 Pct Recovery = 80% Analysis Date = 02/02/15 Pct Recovery = 80% Analysis Date = 01/28/15 Pct Recovery = 80% Analysis Date = 01/28/15 Pct Recovery = 80% Analysis Date = 01/23/15 Pct Recovery = 80% Analysis Date = 01/23/15 Pct Recovery = 80% Analysis Date = 01/18/15 Pct Recovery = 80% Analysis Date = 01/18/15 Pct Recovery = 80% Analysis Date = 01/14/15 Pct Recovery = 80% Analysis Date = 01/14/15 Pct Recovery = 80% Analysis Date = 01/09/15 Pct Recovery = 80% Analysis Date = 01/09/15 Pct Recovery = 80% Analysis Date = 01/04/15 Pct Recovery = 80% Analysis Date = 01/04/15 Pct Recovery = 80% Analysis Date = 12/30/14 Pct Recovery = 80% Analysis Date = 12/30/14 Pct Recovery = 80% Analysis Date = 12/25/14 Pct Recovery = 79% Analysis Date = 12/25/14 Pct Recovery = 79% Analysis Date = 12/21/14 Pct Recovery = 79% Analysis Date = 12/21/14 Pct Recovery = 79% Analysis Date = 12/16/14 Pct Recovery = 79% Analysis Date = 12/16/14 Pct Recovery = 79% Analysis Date = 12/11/14 Pct Recovery = 79% Analysis Date = 12/11/14 Pct Recovery = 79% Analysis Date = 12/06/14 Pct Recovery = 79% Analysis Date = 12/06/14 Pct Recovery = 79% Analysis Date = 12/02/14 Pct Recovery = 79% Analysis Date = 12/02/14 Pct Recovery = 79% Analysis Date = 11/27/14 Pct Recovery = 79% Analysis Date = 11/27/14 Pct Recovery = 79% Analysis Date = 11/22/14 Pct Recovery = 79% Analysis Date = 11/22/14 Pct Recovery = 79% Analysis Date = 11/17/14 Pct Recovery = 78% Analysis Date = 11/17/14 Pct Recovery = 78% Analysis Date = 11/12/14 Pct Recovery = 78% Analysis Date = 11/12/14 Pct Recovery = 78% Analysis Date = 11/08/14 Pct Recovery = 78% Analysis Date = 11/08/14 Pct Recovery = 78% Analysis Date = 11/03/14 Pct Recovery = 78% Analysis Date = 11/03/14 Pct Recovery = 78% Analysis Date = 10/29/14 Pct Recovery = 78% Analysis Date = 10/29/14 Pct Recovery = 78% Analysis Date = 10/24/14 Pct Recovery = 78% Analysis Date = 10/24/14 Pct Recovery = 78% Analysis Date = 10/20/14 Pct Recovery = 78% Analysis Date = 10/20/14 Pct Recovery = 78% Analysis Date = 10/15/14 Pct Recovery = 77% Analysis Date = 10/15/14 Pct Recovery = 77% Analysis Date = 10/10/14 Pct Recovery = 77% Analysis Date = 10/10/14 Pct Recovery = 77% Analysis Date = 10/05/14 Pct Recovery = 77% Analysis Date = 10/05/14 Pct Recovery = 77% Analysis Date = 09/30/14 Pct Recovery = 77% Analysis Date = 09/30/14 Pct Recovery = 77% Analysis Date = 09/26/14 Pct Recovery = 77% Analysis Date = 09/26/14 Pct Recovery = 77% Analysis Date = 09/21/14 Pct Recovery = 77% Analysis Date = 09/21/14 Pct Recovery = 77% Analysis Date = 09/16/14 Pct Recovery = 77% Analysis Date = 09/16/14 Pct Recovery = 77% Analysis Date = 09/11/14 Pct Recovery = 76% Analysis Date = 09/11/14 Pct Recovery = 76% Analysis Date = 09/07/14 Pct Recovery = 76% Analysis Date = 09/07/14 Pct Recovery = 76% Analysis Date = 09/02/14 Pct Recovery = 76% Analysis Date = 09/02/14 Pct Recovery = 76% Analysis Date = 08/28/14 Pct Recovery = 76% Analysis Date = 08/28/14 Pct Recovery = 76% Analysis Date = 08/23/14 Pct Recovery = 76% Analysis Date = 08/23/14 Pct Recovery = 76% Analysis Date = 08/18/14 Pct Recovery = 76% Analysis Date = 08/18/14 Pct Recovery = 76% Analysis Date = 08/14/14 Pct Recovery = 76% Analysis Date = 08/14/14 Pct Recovery = 76% Analysis Date = 08/09/14 Pct Recovery = 75% Analysis Date = 08/09/14 Pct Recovery = 75% Analysis Date = 08/04/14 Pct Recovery = 75% Analysis Date = 08/04/14 Pct Recovery = 75% Analysis Date = 07/30/14 Pct Recovery = 75% Analysis Date = 07/30/14 Pct Recovery = 75% Analysis Date = 07/26/14 Pct Recovery = 75% Analysis Date = 07/26/14 Pct Recovery = 75% Analysis Date = 07/21/14 Pct Recovery = 75% Analysis Date = 07/21/14 Pct Recovery = 75% Analysis Date = 07/16/14 Pct Recovery = 75% Analysis Date = 07/16/14 Pct Recovery = 75% Analysis Date = 07/11/14 Pct Recovery = 75% Analysis Date = 07/11/14 Pct Recovery = 75% Analysis Date = 07/06/14 Pct Recovery = 74% Analysis Date = 07/06/14 Pct Recovery = 74% Analysis Date = 07/02/14 Pct Recovery = 74% Analysis Date = 07/02/14 Pct Recovery = 74% Analysis Date = 06/27/14 Pct Recovery = 74% Analysis Date = 06/27/14 Pct Recovery = 74% Analysis Date = 06/22/14 Pct Recovery = 74% Analysis Date = 06/22/14 Pct Recovery = 74% Analysis Date = 06/17/14 Pct Recovery = 74% Analysis Date = 06/17/14 Pct Recovery = 74% Analysis Date = 06/13/14 Pct Recovery = 74% Analysis Date = 06/13/14 Pct Recovery = 74% Analysis Date = 06/08/14 Pct Recovery = 74% Analysis Date = 06/08/14 Pct Recovery = 74% Analysis Date = 06/03/14 Pct Recovery = 73% Analysis Date = 06/03/14 Pct Recovery = 73% Analysis Date = 05/29/14 Pct Recovery = 73% Analysis Date = 05/29/14 Pct Recovery = 73% Analysis Date = 05/24/14 Pct Recovery = 73% Analysis Date = 05/24/14 Pct Recovery = 73% Analysis Date = 05/20/14 Pct Recovery = 73% Analysis Date = 05/20/14 Pct Recovery = 73% Analysis Date = 05/15/14 Pct Recovery = 73% Analysis Date = 05/15/14 Pct Recovery = 73% Analysis Date = 05/10/14 Pct Recovery = 73% Analysis Date = 05/10/14 Pct Recovery = 73% Analysis Date = 05/05/14 Pct Recovery = 73% Analysis Date = 05/05/14 Pct Recovery = 73% Analysis Date = 05/01/14 Pct Recovery = 72% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
4-ISOPROPYL-1-METHYLBENZENE (CYMENE)

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 49 79% 10% 79% 7%
Total 49 79% 10% 79% 7%

Sample Statistics
4-ISOPROPYL-1-METHYLBENZENE (CYMENE)

Characteristic N % % Basis
Plotted 49 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 49 .  
False Negatives 0 0% 0 out of 49
Not Spiked 24 .  
False Positives 0 0% 0 out of 24

BQS OBSP Determination:
4-METHYL-2-PENTANONE
METHOD: 4440 , TESTIDCODE: 78133GCM66
Open Data Set

Analysis Date = 12/12/16 SpikeMix = Accu 216041125: 40 µl & Crescent 03FF058: 40 µl Pct Recovery = 106% Analysis Date = 08/04/16 SpikeMix = Crescent 03FF058: 40 µl & Supelco LC20141V: 40 µl Pct Recovery = 84% Analysis Date = 11/21/16 SpikeMix = Crescent 03FF058: 25 µl & Supelco LC20141V: 25 µl Pct Recovery = 95% Analysis Date = 06/30/16 SpikeMix = Crescent 03FF058: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 87% Analysis Date = 06/21/16 SpikeMix = Phenova B20160319: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 99% Analysis Date = 05/24/16 SpikeMix = Accu 216041125: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 105% Analysis Date = 09/29/15 SpikeMix = Accu 215041380: 25 µl & ERA 0406-15-03: 25 µl Pct Recovery = 96% Analysis Date = 08/15/15 SpikeMix = Supelco LC13545: 25 µl & Crescent 04EE008: 25 µl Pct Recovery = 99% Analysis Date = 07/13/15 SpikeMix = Crescent 04EE008: 25 µl & NSI 050515AVOC: 25 µl Pct Recovery = 87% Analysis Date = 09/28/16 SpikeMix = Crescent 03FF058: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 90% Analysis Date = 09/08/16 SpikeMix = Phenova B20160319: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 80% Analysis Date = 08/20/16 SpikeMix = Accu 216041125: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 92% Analysis Date = 04/02/16 SpikeMix = Supelco LC13545: 15 µl & Accu 215041380: 15 µl Pct Recovery = 82% Analysis Date = 03/04/16 SpikeMix = Accu 215041380: 15 µl & ERA 0406-15-03: 15 µl Pct Recovery = 85% Analysis Date = 06/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Accu 215041380: 15 µl Pct Recovery = 80% Analysis Date = 12/18/15 SpikeMix = Supelco LC13545: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 98% Analysis Date = 10/17/15 SpikeMix = Crescent 04EE008: 15 µl & NSI 050515AVOC: 15 µl Pct Recovery = 94% Analysis Date = 05/09/15 SpikeMix = Spex Organics EN150428007: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 89% Analysis Date = 02/18/16 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 90% Analysis Date = 11/20/15 SpikeMix = Accu 215041380: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 90% Analysis Date = 11/12/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 84% Analysis Date = 05/21/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 90% Analysis Date = 05/13/16 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 102% Analysis Date = 01/27/16 SpikeMix = Crescent 04EE008: 10 µl & NSI 050515AVOC: 10 µl Pct Recovery = 86% Analysis Date = 07/31/15 SpikeMix = Crescent 04EE008: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 82% Analysis Date = 05/09/15 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 84% Analysis Date = 06/10/14 SpikeMix = Crescent 03DD004: 20 µl & NSI 032614: 20 µl Pct Recovery = 93% Analysis Date = 06/10/14 SpikeMix = NSI 032614: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 100% Analysis Date = 05/01/14 SpikeMix = Accu 214031115: 20 µl & NSI 032614: 20 µl Pct Recovery = 88% Analysis Date = 08/16/14 SpikeMix = ERA 0227-14-06.1A: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 104% Analysis Date = 07/01/14 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 100% Analysis Date = 09/09/14 SpikeMix = Accu 214031115: 10 µl & NSI 032614: 10 µl Pct Recovery = 119% Analysis Date = 09/09/14 SpikeMix = NSI 032614: 10 µl & Spex Organics C1140417015: 10 µl Pct Recovery = 114% Analysis Date = 07/29/14 SpikeMix = Crescent 03DD004: 10 µl & NSI 032614: 10 µl Pct Recovery = 112% Analysis Date = 05/30/14 SpikeMix = NSI 032614: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 82% Analysis Date = 07/11/14 SpikeMix = Spex Organics C1140417015: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 106% Analysis Date = 11/22/14 SpikeMix = NSI 032614: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 94% Analysis Date = 04/09/15 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 99% Analysis Date = 03/06/15 SpikeMix = ERA 0227-14-06.1A: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 106% Analysis Date = 11/14/14 SpikeMix = Crescent 03DD004: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 101% Analysis Date = 01/13/15 SpikeMix = Accu 214031115: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 125% Analysis Date = 10/21/14 SpikeMix = ERA 0227-14-06.1A: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 109% Analysis Date = 10/04/14 SpikeMix = Crescent 03DD004: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 107% Analysis Date = 12/11/16 Pct Recovery = 94% Analysis Date = 12/07/16 Pct Recovery = 94% Analysis Date = 12/07/16 Pct Recovery = 94% Analysis Date = 12/02/16 Pct Recovery = 94% Analysis Date = 12/02/16 Pct Recovery = 94% Analysis Date = 11/27/16 Pct Recovery = 94% Analysis Date = 11/27/16 Pct Recovery = 94% Analysis Date = 11/22/16 Pct Recovery = 94% Analysis Date = 11/22/16 Pct Recovery = 94% Analysis Date = 11/18/16 Pct Recovery = 94% Analysis Date = 11/18/16 Pct Recovery = 94% Analysis Date = 11/13/16 Pct Recovery = 94% Analysis Date = 11/13/16 Pct Recovery = 94% Analysis Date = 11/08/16 Pct Recovery = 94% Analysis Date = 11/08/16 Pct Recovery = 94% Analysis Date = 11/03/16 Pct Recovery = 94% Analysis Date = 11/03/16 Pct Recovery = 94% Analysis Date = 10/29/16 Pct Recovery = 94% Analysis Date = 10/29/16 Pct Recovery = 94% Analysis Date = 10/25/16 Pct Recovery = 94% Analysis Date = 10/25/16 Pct Recovery = 94% Analysis Date = 10/20/16 Pct Recovery = 94% Analysis Date = 10/20/16 Pct Recovery = 94% Analysis Date = 10/15/16 Pct Recovery = 94% Analysis Date = 10/15/16 Pct Recovery = 94% Analysis Date = 10/10/16 Pct Recovery = 94% Analysis Date = 10/10/16 Pct Recovery = 94% Analysis Date = 10/06/16 Pct Recovery = 93% Analysis Date = 10/06/16 Pct Recovery = 93% Analysis Date = 10/01/16 Pct Recovery = 93% Analysis Date = 10/01/16 Pct Recovery = 93% Analysis Date = 09/26/16 Pct Recovery = 93% Analysis Date = 09/26/16 Pct Recovery = 93% Analysis Date = 09/21/16 Pct Recovery = 93% Analysis Date = 09/21/16 Pct Recovery = 93% Analysis Date = 09/16/16 Pct Recovery = 93% Analysis Date = 09/16/16 Pct Recovery = 93% Analysis Date = 09/12/16 Pct Recovery = 93% Analysis Date = 09/12/16 Pct Recovery = 93% Analysis Date = 09/07/16 Pct Recovery = 93% Analysis Date = 09/07/16 Pct Recovery = 93% Analysis Date = 09/02/16 Pct Recovery = 93% Analysis Date = 09/02/16 Pct Recovery = 93% Analysis Date = 08/28/16 Pct Recovery = 93% Analysis Date = 08/28/16 Pct Recovery = 93% Analysis Date = 08/24/16 Pct Recovery = 93% Analysis Date = 08/24/16 Pct Recovery = 93% Analysis Date = 08/19/16 Pct Recovery = 93% Analysis Date = 08/19/16 Pct Recovery = 93% Analysis Date = 08/14/16 Pct Recovery = 93% Analysis Date = 08/14/16 Pct Recovery = 93% Analysis Date = 08/09/16 Pct Recovery = 93% Analysis Date = 08/09/16 Pct Recovery = 93% Analysis Date = 08/04/16 Pct Recovery = 93% Analysis Date = 08/04/16 Pct Recovery = 93% Analysis Date = 07/31/16 Pct Recovery = 93% Analysis Date = 07/31/16 Pct Recovery = 93% Analysis Date = 07/26/16 Pct Recovery = 93% Analysis Date = 07/26/16 Pct Recovery = 93% Analysis Date = 07/21/16 Pct Recovery = 93% Analysis Date = 07/21/16 Pct Recovery = 93% Analysis Date = 07/16/16 Pct Recovery = 92% Analysis Date = 07/16/16 Pct Recovery = 92% Analysis Date = 07/12/16 Pct Recovery = 92% Analysis Date = 07/12/16 Pct Recovery = 92% Analysis Date = 07/07/16 Pct Recovery = 92% Analysis Date = 07/07/16 Pct Recovery = 92% Analysis Date = 07/02/16 Pct Recovery = 92% Analysis Date = 07/02/16 Pct Recovery = 92% Analysis Date = 06/27/16 Pct Recovery = 92% Analysis Date = 06/27/16 Pct Recovery = 92% Analysis Date = 06/22/16 Pct Recovery = 92% Analysis Date = 06/22/16 Pct Recovery = 92% Analysis Date = 06/18/16 Pct Recovery = 92% Analysis Date = 06/18/16 Pct Recovery = 92% Analysis Date = 06/13/16 Pct Recovery = 92% Analysis Date = 06/13/16 Pct Recovery = 92% Analysis Date = 06/08/16 Pct Recovery = 92% Analysis Date = 06/08/16 Pct Recovery = 92% Analysis Date = 06/03/16 Pct Recovery = 92% Analysis Date = 06/03/16 Pct Recovery = 92% Analysis Date = 05/30/16 Pct Recovery = 92% Analysis Date = 05/30/16 Pct Recovery = 92% Analysis Date = 05/25/16 Pct Recovery = 92% Analysis Date = 05/25/16 Pct Recovery = 92% Analysis Date = 05/20/16 Pct Recovery = 92% Analysis Date = 05/20/16 Pct Recovery = 92% Analysis Date = 05/15/16 Pct Recovery = 92% Analysis Date = 05/15/16 Pct Recovery = 92% Analysis Date = 05/10/16 Pct Recovery = 92% Analysis Date = 05/10/16 Pct Recovery = 92% Analysis Date = 05/06/16 Pct Recovery = 92% Analysis Date = 05/06/16 Pct Recovery = 92% Analysis Date = 05/01/16 Pct Recovery = 92% Analysis Date = 05/01/16 Pct Recovery = 92% Analysis Date = 04/26/16 Pct Recovery = 92% Analysis Date = 04/26/16 Pct Recovery = 92% Analysis Date = 04/21/16 Pct Recovery = 91% Analysis Date = 04/21/16 Pct Recovery = 91% Analysis Date = 04/16/16 Pct Recovery = 91% Analysis Date = 04/16/16 Pct Recovery = 91% Analysis Date = 04/12/16 Pct Recovery = 91% Analysis Date = 04/12/16 Pct Recovery = 91% Analysis Date = 04/07/16 Pct Recovery = 91% Analysis Date = 04/07/16 Pct Recovery = 91% Analysis Date = 04/02/16 Pct Recovery = 91% Analysis Date = 04/02/16 Pct Recovery = 91% Analysis Date = 03/28/16 Pct Recovery = 91% Analysis Date = 03/28/16 Pct Recovery = 91% Analysis Date = 03/24/16 Pct Recovery = 91% Analysis Date = 03/24/16 Pct Recovery = 91% Analysis Date = 03/19/16 Pct Recovery = 91% Analysis Date = 03/19/16 Pct Recovery = 91% Analysis Date = 03/14/16 Pct Recovery = 91% Analysis Date = 03/14/16 Pct Recovery = 91% Analysis Date = 03/09/16 Pct Recovery = 91% Analysis Date = 03/09/16 Pct Recovery = 91% Analysis Date = 03/04/16 Pct Recovery = 91% Analysis Date = 03/04/16 Pct Recovery = 91% Analysis Date = 02/29/16 Pct Recovery = 91% Analysis Date = 02/29/16 Pct Recovery = 91% Analysis Date = 02/24/16 Pct Recovery = 91% Analysis Date = 02/24/16 Pct Recovery = 91% Analysis Date = 02/19/16 Pct Recovery = 91% Analysis Date = 02/19/16 Pct Recovery = 91% Analysis Date = 02/14/16 Pct Recovery = 91% Analysis Date = 02/14/16 Pct Recovery = 91% Analysis Date = 02/10/16 Pct Recovery = 91% Analysis Date = 02/10/16 Pct Recovery = 91% Analysis Date = 02/05/16 Pct Recovery = 91% Analysis Date = 02/05/16 Pct Recovery = 91% Analysis Date = 01/31/16 Pct Recovery = 91% Analysis Date = 01/31/16 Pct Recovery = 91% Analysis Date = 01/26/16 Pct Recovery = 91% Analysis Date = 01/26/16 Pct Recovery = 91% Analysis Date = 01/21/16 Pct Recovery = 91% Analysis Date = 01/21/16 Pct Recovery = 91% Analysis Date = 01/17/16 Pct Recovery = 91% Analysis Date = 01/17/16 Pct Recovery = 91% Analysis Date = 01/12/16 Pct Recovery = 91% Analysis Date = 01/12/16 Pct Recovery = 91% Analysis Date = 01/07/16 Pct Recovery = 91% Analysis Date = 01/07/16 Pct Recovery = 91% Analysis Date = 01/02/16 Pct Recovery = 91% Analysis Date = 01/02/16 Pct Recovery = 91% Analysis Date = 12/29/15 Pct Recovery = 91% Analysis Date = 12/29/15 Pct Recovery = 91% Analysis Date = 12/24/15 Pct Recovery = 91% Analysis Date = 12/24/15 Pct Recovery = 91% Analysis Date = 12/19/15 Pct Recovery = 91% Analysis Date = 12/19/15 Pct Recovery = 91% Analysis Date = 12/14/15 Pct Recovery = 91% Analysis Date = 12/14/15 Pct Recovery = 91% Analysis Date = 12/09/15 Pct Recovery = 91% Analysis Date = 12/09/15 Pct Recovery = 91% Analysis Date = 12/05/15 Pct Recovery = 91% Analysis Date = 12/05/15 Pct Recovery = 91% Analysis Date = 11/30/15 Pct Recovery = 91% Analysis Date = 11/30/15 Pct Recovery = 91% Analysis Date = 11/25/15 Pct Recovery = 90% Analysis Date = 11/25/15 Pct Recovery = 90% Analysis Date = 11/20/15 Pct Recovery = 90% Analysis Date = 11/20/15 Pct Recovery = 90% Analysis Date = 11/16/15 Pct Recovery = 90% Analysis Date = 11/16/15 Pct Recovery = 90% Analysis Date = 11/11/15 Pct Recovery = 90% Analysis Date = 11/11/15 Pct Recovery = 90% Analysis Date = 11/06/15 Pct Recovery = 90% Analysis Date = 11/06/15 Pct Recovery = 90% Analysis Date = 11/01/15 Pct Recovery = 90% Analysis Date = 11/01/15 Pct Recovery = 90% Analysis Date = 10/27/15 Pct Recovery = 90% Analysis Date = 10/27/15 Pct Recovery = 90% Analysis Date = 10/23/15 Pct Recovery = 90% Analysis Date = 10/23/15 Pct Recovery = 90% Analysis Date = 10/18/15 Pct Recovery = 90% Analysis Date = 10/18/15 Pct Recovery = 90% Analysis Date = 10/13/15 Pct Recovery = 90% Analysis Date = 10/13/15 Pct Recovery = 90% Analysis Date = 10/08/15 Pct Recovery = 90% Analysis Date = 10/08/15 Pct Recovery = 90% Analysis Date = 10/04/15 Pct Recovery = 90% Analysis Date = 10/04/15 Pct Recovery = 90% Analysis Date = 09/29/15 Pct Recovery = 90% Analysis Date = 09/29/15 Pct Recovery = 90% Analysis Date = 09/24/15 Pct Recovery = 90% Analysis Date = 09/24/15 Pct Recovery = 90% Analysis Date = 09/19/15 Pct Recovery = 91% Analysis Date = 09/19/15 Pct Recovery = 91% Analysis Date = 09/14/15 Pct Recovery = 91% Analysis Date = 09/14/15 Pct Recovery = 91% Analysis Date = 09/10/15 Pct Recovery = 91% Analysis Date = 09/10/15 Pct Recovery = 91% Analysis Date = 09/05/15 Pct Recovery = 91% Analysis Date = 09/05/15 Pct Recovery = 91% Analysis Date = 08/31/15 Pct Recovery = 91% Analysis Date = 08/31/15 Pct Recovery = 91% Analysis Date = 08/26/15 Pct Recovery = 91% Analysis Date = 08/26/15 Pct Recovery = 91% Analysis Date = 08/21/15 Pct Recovery = 91% Analysis Date = 08/21/15 Pct Recovery = 91% Analysis Date = 08/17/15 Pct Recovery = 91% Analysis Date = 08/17/15 Pct Recovery = 91% Analysis Date = 08/12/15 Pct Recovery = 92% Analysis Date = 08/12/15 Pct Recovery = 92% Analysis Date = 08/07/15 Pct Recovery = 92% Analysis Date = 08/07/15 Pct Recovery = 92% Analysis Date = 08/02/15 Pct Recovery = 92% Analysis Date = 08/02/15 Pct Recovery = 92% Analysis Date = 07/29/15 Pct Recovery = 92% Analysis Date = 07/29/15 Pct Recovery = 92% Analysis Date = 07/24/15 Pct Recovery = 92% Analysis Date = 07/24/15 Pct Recovery = 92% Analysis Date = 07/19/15 Pct Recovery = 92% Analysis Date = 07/19/15 Pct Recovery = 92% Analysis Date = 07/14/15 Pct Recovery = 92% Analysis Date = 07/14/15 Pct Recovery = 92% Analysis Date = 07/09/15 Pct Recovery = 92% Analysis Date = 07/09/15 Pct Recovery = 92% Analysis Date = 07/05/15 Pct Recovery = 93% Analysis Date = 07/05/15 Pct Recovery = 93% Analysis Date = 06/30/15 Pct Recovery = 93% Analysis Date = 06/30/15 Pct Recovery = 93% Analysis Date = 06/25/15 Pct Recovery = 93% Analysis Date = 06/25/15 Pct Recovery = 93% Analysis Date = 06/20/15 Pct Recovery = 93% Analysis Date = 06/20/15 Pct Recovery = 93% Analysis Date = 06/16/15 Pct Recovery = 93% Analysis Date = 06/16/15 Pct Recovery = 93% Analysis Date = 06/11/15 Pct Recovery = 94% Analysis Date = 06/11/15 Pct Recovery = 94% Analysis Date = 06/06/15 Pct Recovery = 94% Analysis Date = 06/06/15 Pct Recovery = 94% Analysis Date = 06/01/15 Pct Recovery = 94% Analysis Date = 06/01/15 Pct Recovery = 94% Analysis Date = 05/27/15 Pct Recovery = 94% Analysis Date = 05/27/15 Pct Recovery = 94% Analysis Date = 05/23/15 Pct Recovery = 94% Analysis Date = 05/23/15 Pct Recovery = 94% Analysis Date = 05/18/15 Pct Recovery = 95% Analysis Date = 05/18/15 Pct Recovery = 95% Analysis Date = 05/13/15 Pct Recovery = 95% Analysis Date = 05/13/15 Pct Recovery = 95% Analysis Date = 05/08/15 Pct Recovery = 95% Analysis Date = 05/08/15 Pct Recovery = 95% Analysis Date = 05/04/15 Pct Recovery = 95% Analysis Date = 05/04/15 Pct Recovery = 95% Analysis Date = 04/29/15 Pct Recovery = 95% Analysis Date = 04/29/15 Pct Recovery = 95% Analysis Date = 04/24/15 Pct Recovery = 96% Analysis Date = 04/24/15 Pct Recovery = 96% Analysis Date = 04/19/15 Pct Recovery = 96% Analysis Date = 04/19/15 Pct Recovery = 96% Analysis Date = 04/14/15 Pct Recovery = 96% Analysis Date = 04/14/15 Pct Recovery = 96% Analysis Date = 04/10/15 Pct Recovery = 96% Analysis Date = 04/10/15 Pct Recovery = 96% Analysis Date = 04/05/15 Pct Recovery = 96% Analysis Date = 04/05/15 Pct Recovery = 96% Analysis Date = 03/31/15 Pct Recovery = 97% Analysis Date = 03/31/15 Pct Recovery = 97% Analysis Date = 03/26/15 Pct Recovery = 97% Analysis Date = 03/26/15 Pct Recovery = 97% Analysis Date = 03/22/15 Pct Recovery = 97% Analysis Date = 03/22/15 Pct Recovery = 97% Analysis Date = 03/17/15 Pct Recovery = 97% Analysis Date = 03/17/15 Pct Recovery = 97% Analysis Date = 03/12/15 Pct Recovery = 97% Analysis Date = 03/12/15 Pct Recovery = 97% Analysis Date = 03/07/15 Pct Recovery = 98% Analysis Date = 03/07/15 Pct Recovery = 98% Analysis Date = 03/02/15 Pct Recovery = 98% Analysis Date = 03/02/15 Pct Recovery = 98% Analysis Date = 02/26/15 Pct Recovery = 98% Analysis Date = 02/26/15 Pct Recovery = 98% Analysis Date = 02/21/15 Pct Recovery = 98% Analysis Date = 02/21/15 Pct Recovery = 98% Analysis Date = 02/16/15 Pct Recovery = 98% Analysis Date = 02/16/15 Pct Recovery = 98% Analysis Date = 02/11/15 Pct Recovery = 99% Analysis Date = 02/11/15 Pct Recovery = 99% Analysis Date = 02/07/15 Pct Recovery = 99% Analysis Date = 02/07/15 Pct Recovery = 99% Analysis Date = 02/02/15 Pct Recovery = 99% Analysis Date = 02/02/15 Pct Recovery = 99% Analysis Date = 01/28/15 Pct Recovery = 99% Analysis Date = 01/28/15 Pct Recovery = 99% Analysis Date = 01/23/15 Pct Recovery = 99% Analysis Date = 01/23/15 Pct Recovery = 99% Analysis Date = 01/18/15 Pct Recovery = 99% Analysis Date = 01/18/15 Pct Recovery = 99% Analysis Date = 01/14/15 Pct Recovery = 100% Analysis Date = 01/14/15 Pct Recovery = 100% Analysis Date = 01/09/15 Pct Recovery = 100% Analysis Date = 01/09/15 Pct Recovery = 100% Analysis Date = 01/04/15 Pct Recovery = 100% Analysis Date = 01/04/15 Pct Recovery = 100% Analysis Date = 12/30/14 Pct Recovery = 100% Analysis Date = 12/30/14 Pct Recovery = 100% Analysis Date = 12/25/14 Pct Recovery = 100% Analysis Date = 12/25/14 Pct Recovery = 100% Analysis Date = 12/21/14 Pct Recovery = 101% Analysis Date = 12/21/14 Pct Recovery = 101% Analysis Date = 12/16/14 Pct Recovery = 101% Analysis Date = 12/16/14 Pct Recovery = 101% Analysis Date = 12/11/14 Pct Recovery = 101% Analysis Date = 12/11/14 Pct Recovery = 101% Analysis Date = 12/06/14 Pct Recovery = 101% Analysis Date = 12/06/14 Pct Recovery = 101% Analysis Date = 12/02/14 Pct Recovery = 101% Analysis Date = 12/02/14 Pct Recovery = 101% Analysis Date = 11/27/14 Pct Recovery = 102% Analysis Date = 11/27/14 Pct Recovery = 102% Analysis Date = 11/22/14 Pct Recovery = 102% Analysis Date = 11/22/14 Pct Recovery = 102% Analysis Date = 11/17/14 Pct Recovery = 102% Analysis Date = 11/17/14 Pct Recovery = 102% Analysis Date = 11/12/14 Pct Recovery = 102% Analysis Date = 11/12/14 Pct Recovery = 102% Analysis Date = 11/08/14 Pct Recovery = 102% Analysis Date = 11/08/14 Pct Recovery = 102% Analysis Date = 11/03/14 Pct Recovery = 102% Analysis Date = 11/03/14 Pct Recovery = 102% Analysis Date = 10/29/14 Pct Recovery = 102% Analysis Date = 10/29/14 Pct Recovery = 102% Analysis Date = 10/24/14 Pct Recovery = 102% Analysis Date = 10/24/14 Pct Recovery = 102% Analysis Date = 10/20/14 Pct Recovery = 102% Analysis Date = 10/20/14 Pct Recovery = 102% Analysis Date = 10/15/14 Pct Recovery = 102% Analysis Date = 10/15/14 Pct Recovery = 102% Analysis Date = 10/10/14 Pct Recovery = 102% Analysis Date = 10/10/14 Pct Recovery = 102% Analysis Date = 10/05/14 Pct Recovery = 102% Analysis Date = 10/05/14 Pct Recovery = 102% Analysis Date = 09/30/14 Pct Recovery = 102% Analysis Date = 09/30/14 Pct Recovery = 102% Analysis Date = 09/26/14 Pct Recovery = 102% Analysis Date = 09/26/14 Pct Recovery = 102% Analysis Date = 09/21/14 Pct Recovery = 102% Analysis Date = 09/21/14 Pct Recovery = 102% Analysis Date = 09/16/14 Pct Recovery = 102% Analysis Date = 09/16/14 Pct Recovery = 102% Analysis Date = 09/11/14 Pct Recovery = 102% Analysis Date = 09/11/14 Pct Recovery = 102% Analysis Date = 09/07/14 Pct Recovery = 102% Analysis Date = 09/07/14 Pct Recovery = 102% Analysis Date = 09/02/14 Pct Recovery = 102% Analysis Date = 09/02/14 Pct Recovery = 102% Analysis Date = 08/28/14 Pct Recovery = 102% Analysis Date = 08/28/14 Pct Recovery = 102% Analysis Date = 08/23/14 Pct Recovery = 102% Analysis Date = 08/23/14 Pct Recovery = 102% Analysis Date = 08/18/14 Pct Recovery = 102% Analysis Date = 08/18/14 Pct Recovery = 102% Analysis Date = 08/14/14 Pct Recovery = 102% Analysis Date = 08/14/14 Pct Recovery = 102% Analysis Date = 08/09/14 Pct Recovery = 102% Analysis Date = 08/09/14 Pct Recovery = 102% Analysis Date = 08/04/14 Pct Recovery = 102% Analysis Date = 08/04/14 Pct Recovery = 102% Analysis Date = 07/30/14 Pct Recovery = 102% Analysis Date = 07/30/14 Pct Recovery = 102% Analysis Date = 07/26/14 Pct Recovery = 102% Analysis Date = 07/26/14 Pct Recovery = 102% Analysis Date = 07/21/14 Pct Recovery = 102% Analysis Date = 07/21/14 Pct Recovery = 102% Analysis Date = 07/16/14 Pct Recovery = 102% Analysis Date = 07/16/14 Pct Recovery = 102% Analysis Date = 07/11/14 Pct Recovery = 102% Analysis Date = 07/11/14 Pct Recovery = 102% Analysis Date = 07/06/14 Pct Recovery = 101% Analysis Date = 07/06/14 Pct Recovery = 101% Analysis Date = 07/02/14 Pct Recovery = 101% Analysis Date = 07/02/14 Pct Recovery = 101% Analysis Date = 06/27/14 Pct Recovery = 101% Analysis Date = 06/27/14 Pct Recovery = 101% Analysis Date = 06/22/14 Pct Recovery = 101% Analysis Date = 06/22/14 Pct Recovery = 101% Analysis Date = 06/17/14 Pct Recovery = 101% Analysis Date = 06/17/14 Pct Recovery = 101% Analysis Date = 06/13/14 Pct Recovery = 101% Analysis Date = 06/13/14 Pct Recovery = 101% Analysis Date = 06/08/14 Pct Recovery = 101% Analysis Date = 06/08/14 Pct Recovery = 101% Analysis Date = 06/03/14 Pct Recovery = 101% Analysis Date = 06/03/14 Pct Recovery = 101% Analysis Date = 05/29/14 Pct Recovery = 101% Analysis Date = 05/29/14 Pct Recovery = 101% Analysis Date = 05/24/14 Pct Recovery = 101% Analysis Date = 05/24/14 Pct Recovery = 101% Analysis Date = 05/20/14 Pct Recovery = 101% Analysis Date = 05/20/14 Pct Recovery = 101% Analysis Date = 05/15/14 Pct Recovery = 100% Analysis Date = 05/15/14 Pct Recovery = 100% Analysis Date = 05/10/14 Pct Recovery = 100% Analysis Date = 05/10/14 Pct Recovery = 100% Analysis Date = 05/05/14 Pct Recovery = 100% Analysis Date = 05/05/14 Pct Recovery = 100% Analysis Date = 05/01/14 Pct Recovery = 100% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
4-METHYL-2-PENTANONE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 7 106% 10% 106% 8%
>= Reporting Level 36 94% 10% 91% 11%
Total 43 96% 11% 94% 12%

Sample Statistics
4-METHYL-2-PENTANONE

Characteristic N % % Basis
Plotted 43 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 43 .  
False Negatives 0 0% 0 out of 43
Not Spiked 23 .  
False Positives 0 0% 0 out of 23

BQS OBSP Determination:
ACETONE
METHOD: 4440 , TESTIDCODE: 81552GCM66
Open Data Set

Analysis Date = 12/12/16 SpikeMix = Accu 216041125: 40 µl & Crescent 03FF058: 40 µl Pct Recovery = 127% Analysis Date = 07/20/16 SpikeMix = Supelco LC20141V: 40 µl & Accu 216041125: 40 µl Pct Recovery = 116% Analysis Date = 07/14/16 SpikeMix = Accu 216041125: 40 µl & NSI 041816AVOC: 40 µl Pct Recovery = 98% Analysis Date = 09/08/16 SpikeMix = Supelco LC20141V: 25 µl & Accu 216041125: 25 µl Pct Recovery = 107% Analysis Date = 05/24/16 SpikeMix = Accu 216041125: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 108% Analysis Date = 08/12/16 SpikeMix = ChemService 5082900: 25 µl & Phenova B20160319: 25 µl Pct Recovery = 109% Analysis Date = 06/21/16 SpikeMix = Phenova B20160319: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 115% Analysis Date = 07/13/15 SpikeMix = Crescent 04EE008: 25 µl & NSI 050515AVOC: 25 µl Pct Recovery = 129% Analysis Date = 09/29/15 SpikeMix = Accu 215041380: 25 µl & ERA 0406-15-03: 25 µl Pct Recovery = 111% Analysis Date = 06/16/15 SpikeMix = ERA 0406-15-03: 25 µl & Supelco LC13545: 25 µl Pct Recovery = 92% Analysis Date = 04/09/15 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 105% Analysis Date = 08/19/14 SpikeMix = Spex Organics C1140417015: 20 µl & Accu 214031115: 20 µl Pct Recovery = 135% Analysis Date = 07/01/14 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 126% Analysis Date = 05/01/14 SpikeMix = Accu 214031115: 20 µl & NSI 032614: 20 µl Pct Recovery = 124% Analysis Date = 03/19/15 SpikeMix = Spex Organics C1140417015: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 109% Analysis Date = 12/17/14 SpikeMix = Supelco LC06438: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 112% Analysis Date = 11/14/14 SpikeMix = Crescent 03DD004: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 106% Analysis Date = 06/10/14 SpikeMix = Crescent 03DD004: 20 µl & NSI 032614: 20 µl Pct Recovery = 127% Analysis Date = 10/13/16 SpikeMix = Accu 216041125: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 124% Analysis Date = 08/20/16 SpikeMix = Accu 216041125: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 138% Analysis Date = 06/30/16 SpikeMix = ChemService 5082900: 15 µl & Accu 216041125: 15 µl Pct Recovery = 80% Analysis Date = 11/29/16 SpikeMix = ChemService 5082900: 15 µl & Phenova B20160319: 15 µl Pct Recovery = 104% Analysis Date = 09/08/16 SpikeMix = Phenova B20160319: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 116% Analysis Date = 07/29/16 SpikeMix = Phenova B20160319: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 98% Analysis Date = 05/27/16 SpikeMix = Phenova B20160319: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 106% Analysis Date = 11/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 117% Analysis Date = 10/17/15 SpikeMix = Crescent 04EE008: 15 µl & NSI 050515AVOC: 15 µl Pct Recovery = 102% Analysis Date = 06/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Accu 215041380: 15 µl Pct Recovery = 99% Analysis Date = 04/26/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 115% Analysis Date = 03/04/16 SpikeMix = Accu 215041380: 15 µl & ERA 0406-15-03: 15 µl Pct Recovery = 122% Analysis Date = 02/05/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 99% Analysis Date = 10/16/15 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 107% Analysis Date = 01/24/15 SpikeMix = Accu 214031115: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 115% Analysis Date = 09/09/14 SpikeMix = Accu 214031115: 10 µl & NSI 032614: 10 µl Pct Recovery = 175% Analysis Date = 07/23/14 SpikeMix = Spex Organics C1140417015: 10 µl & Accu 214031115: 10 µl Pct Recovery = 133% Analysis Date = 06/18/14 SpikeMix = Supelco LC06438: 10 µl & Accu 214031115: 10 µl Pct Recovery = 120% Analysis Date = 11/06/14 SpikeMix = Spex Organics C1140417015: 10 µl & Crescent 03DD004: 10 µl Pct Recovery = 114% Analysis Date = 10/04/14 SpikeMix = Crescent 03DD004: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 85% Analysis Date = 07/29/14 SpikeMix = Crescent 03DD004: 10 µl & NSI 032614: 10 µl Pct Recovery = 116% Analysis Date = 05/03/14 SpikeMix = Crescent 03DD004: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 127% Analysis Date = 03/17/16 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 114% Analysis Date = 01/27/16 SpikeMix = Crescent 04EE008: 10 µl & NSI 050515AVOC: 10 µl Pct Recovery = 91% Analysis Date = 12/10/15 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 115% Analysis Date = 09/03/15 SpikeMix = NSI 050515AVOC: 10 µl & Spex Organics EN150428007: 10 µl Pct Recovery = 92% Analysis Date = 11/20/15 SpikeMix = Accu 215041380: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 118% Analysis Date = 07/31/15 SpikeMix = Crescent 04EE008: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 107% Analysis Date = 06/27/15 SpikeMix = ERA 0406-15-03: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 119% Analysis Date = 12/11/16 Pct Recovery = 115% Analysis Date = 12/07/16 Pct Recovery = 115% Analysis Date = 12/07/16 Pct Recovery = 115% Analysis Date = 12/02/16 Pct Recovery = 115% Analysis Date = 12/02/16 Pct Recovery = 115% Analysis Date = 11/27/16 Pct Recovery = 115% Analysis Date = 11/27/16 Pct Recovery = 115% Analysis Date = 11/22/16 Pct Recovery = 115% Analysis Date = 11/22/16 Pct Recovery = 115% Analysis Date = 11/18/16 Pct Recovery = 115% Analysis Date = 11/18/16 Pct Recovery = 115% Analysis Date = 11/13/16 Pct Recovery = 114% Analysis Date = 11/13/16 Pct Recovery = 114% Analysis Date = 11/08/16 Pct Recovery = 114% Analysis Date = 11/08/16 Pct Recovery = 114% Analysis Date = 11/03/16 Pct Recovery = 114% Analysis Date = 11/03/16 Pct Recovery = 114% Analysis Date = 10/29/16 Pct Recovery = 114% Analysis Date = 10/29/16 Pct Recovery = 114% Analysis Date = 10/25/16 Pct Recovery = 114% Analysis Date = 10/25/16 Pct Recovery = 114% Analysis Date = 10/20/16 Pct Recovery = 114% Analysis Date = 10/20/16 Pct Recovery = 114% Analysis Date = 10/15/16 Pct Recovery = 113% Analysis Date = 10/15/16 Pct Recovery = 113% Analysis Date = 10/10/16 Pct Recovery = 113% Analysis Date = 10/10/16 Pct Recovery = 113% Analysis Date = 10/06/16 Pct Recovery = 113% Analysis Date = 10/06/16 Pct Recovery = 113% Analysis Date = 10/01/16 Pct Recovery = 113% Analysis Date = 10/01/16 Pct Recovery = 113% Analysis Date = 09/26/16 Pct Recovery = 113% Analysis Date = 09/26/16 Pct Recovery = 113% Analysis Date = 09/21/16 Pct Recovery = 113% Analysis Date = 09/21/16 Pct Recovery = 113% Analysis Date = 09/16/16 Pct Recovery = 113% Analysis Date = 09/16/16 Pct Recovery = 113% Analysis Date = 09/12/16 Pct Recovery = 112% Analysis Date = 09/12/16 Pct Recovery = 112% Analysis Date = 09/07/16 Pct Recovery = 112% Analysis Date = 09/07/16 Pct Recovery = 112% Analysis Date = 09/02/16 Pct Recovery = 112% Analysis Date = 09/02/16 Pct Recovery = 112% Analysis Date = 08/28/16 Pct Recovery = 112% Analysis Date = 08/28/16 Pct Recovery = 112% Analysis Date = 08/24/16 Pct Recovery = 112% Analysis Date = 08/24/16 Pct Recovery = 112% Analysis Date = 08/19/16 Pct Recovery = 112% Analysis Date = 08/19/16 Pct Recovery = 112% Analysis Date = 08/14/16 Pct Recovery = 112% Analysis Date = 08/14/16 Pct Recovery = 112% Analysis Date = 08/09/16 Pct Recovery = 112% Analysis Date = 08/09/16 Pct Recovery = 112% Analysis Date = 08/04/16 Pct Recovery = 111% Analysis Date = 08/04/16 Pct Recovery = 111% Analysis Date = 07/31/16 Pct Recovery = 111% Analysis Date = 07/31/16 Pct Recovery = 111% Analysis Date = 07/26/16 Pct Recovery = 111% Analysis Date = 07/26/16 Pct Recovery = 111% Analysis Date = 07/21/16 Pct Recovery = 111% Analysis Date = 07/21/16 Pct Recovery = 111% Analysis Date = 07/16/16 Pct Recovery = 111% Analysis Date = 07/16/16 Pct Recovery = 111% Analysis Date = 07/12/16 Pct Recovery = 111% Analysis Date = 07/12/16 Pct Recovery = 111% Analysis Date = 07/07/16 Pct Recovery = 111% Analysis Date = 07/07/16 Pct Recovery = 111% Analysis Date = 07/02/16 Pct Recovery = 111% Analysis Date = 07/02/16 Pct Recovery = 111% Analysis Date = 06/27/16 Pct Recovery = 110% Analysis Date = 06/27/16 Pct Recovery = 110% Analysis Date = 06/22/16 Pct Recovery = 110% Analysis Date = 06/22/16 Pct Recovery = 110% Analysis Date = 06/18/16 Pct Recovery = 110% Analysis Date = 06/18/16 Pct Recovery = 110% Analysis Date = 06/13/16 Pct Recovery = 110% Analysis Date = 06/13/16 Pct Recovery = 110% Analysis Date = 06/08/16 Pct Recovery = 110% Analysis Date = 06/08/16 Pct Recovery = 110% Analysis Date = 06/03/16 Pct Recovery = 110% Analysis Date = 06/03/16 Pct Recovery = 110% Analysis Date = 05/30/16 Pct Recovery = 110% Analysis Date = 05/30/16 Pct Recovery = 110% Analysis Date = 05/25/16 Pct Recovery = 110% Analysis Date = 05/25/16 Pct Recovery = 110% Analysis Date = 05/20/16 Pct Recovery = 110% Analysis Date = 05/20/16 Pct Recovery = 110% Analysis Date = 05/15/16 Pct Recovery = 110% Analysis Date = 05/15/16 Pct Recovery = 110% Analysis Date = 05/10/16 Pct Recovery = 109% Analysis Date = 05/10/16 Pct Recovery = 109% Analysis Date = 05/06/16 Pct Recovery = 109% Analysis Date = 05/06/16 Pct Recovery = 109% Analysis Date = 05/01/16 Pct Recovery = 109% Analysis Date = 05/01/16 Pct Recovery = 109% Analysis Date = 04/26/16 Pct Recovery = 109% Analysis Date = 04/26/16 Pct Recovery = 109% Analysis Date = 04/21/16 Pct Recovery = 109% Analysis Date = 04/21/16 Pct Recovery = 109% Analysis Date = 04/16/16 Pct Recovery = 109% Analysis Date = 04/16/16 Pct Recovery = 109% Analysis Date = 04/12/16 Pct Recovery = 109% Analysis Date = 04/12/16 Pct Recovery = 109% Analysis Date = 04/07/16 Pct Recovery = 109% Analysis Date = 04/07/16 Pct Recovery = 109% Analysis Date = 04/02/16 Pct Recovery = 109% Analysis Date = 04/02/16 Pct Recovery = 109% Analysis Date = 03/28/16 Pct Recovery = 109% Analysis Date = 03/28/16 Pct Recovery = 109% Analysis Date = 03/24/16 Pct Recovery = 109% Analysis Date = 03/24/16 Pct Recovery = 109% Analysis Date = 03/19/16 Pct Recovery = 109% Analysis Date = 03/19/16 Pct Recovery = 109% Analysis Date = 03/14/16 Pct Recovery = 109% Analysis Date = 03/14/16 Pct Recovery = 109% Analysis Date = 03/09/16 Pct Recovery = 109% Analysis Date = 03/09/16 Pct Recovery = 109% Analysis Date = 03/04/16 Pct Recovery = 109% Analysis Date = 03/04/16 Pct Recovery = 109% Analysis Date = 02/29/16 Pct Recovery = 109% Analysis Date = 02/29/16 Pct Recovery = 109% Analysis Date = 02/24/16 Pct Recovery = 109% Analysis Date = 02/24/16 Pct Recovery = 109% Analysis Date = 02/19/16 Pct Recovery = 109% Analysis Date = 02/19/16 Pct Recovery = 109% Analysis Date = 02/14/16 Pct Recovery = 108% Analysis Date = 02/14/16 Pct Recovery = 108% Analysis Date = 02/10/16 Pct Recovery = 108% Analysis Date = 02/10/16 Pct Recovery = 108% Analysis Date = 02/05/16 Pct Recovery = 108% Analysis Date = 02/05/16 Pct Recovery = 108% Analysis Date = 01/31/16 Pct Recovery = 108% Analysis Date = 01/31/16 Pct Recovery = 108% Analysis Date = 01/26/16 Pct Recovery = 108% Analysis Date = 01/26/16 Pct Recovery = 108% Analysis Date = 01/21/16 Pct Recovery = 108% Analysis Date = 01/21/16 Pct Recovery = 108% Analysis Date = 01/17/16 Pct Recovery = 108% Analysis Date = 01/17/16 Pct Recovery = 108% Analysis Date = 01/12/16 Pct Recovery = 108% Analysis Date = 01/12/16 Pct Recovery = 108% Analysis Date = 01/07/16 Pct Recovery = 108% Analysis Date = 01/07/16 Pct Recovery = 108% Analysis Date = 01/02/16 Pct Recovery = 108% Analysis Date = 01/02/16 Pct Recovery = 108% Analysis Date = 12/29/15 Pct Recovery = 109% Analysis Date = 12/29/15 Pct Recovery = 109% Analysis Date = 12/24/15 Pct Recovery = 109% Analysis Date = 12/24/15 Pct Recovery = 109% Analysis Date = 12/19/15 Pct Recovery = 109% Analysis Date = 12/19/15 Pct Recovery = 109% Analysis Date = 12/14/15 Pct Recovery = 109% Analysis Date = 12/14/15 Pct Recovery = 109% Analysis Date = 12/09/15 Pct Recovery = 109% Analysis Date = 12/09/15 Pct Recovery = 109% Analysis Date = 12/05/15 Pct Recovery = 109% Analysis Date = 12/05/15 Pct Recovery = 109% Analysis Date = 11/30/15 Pct Recovery = 109% Analysis Date = 11/30/15 Pct Recovery = 109% Analysis Date = 11/25/15 Pct Recovery = 109% Analysis Date = 11/25/15 Pct Recovery = 109% Analysis Date = 11/20/15 Pct Recovery = 109% Analysis Date = 11/20/15 Pct Recovery = 109% Analysis Date = 11/16/15 Pct Recovery = 109% Analysis Date = 11/16/15 Pct Recovery = 109% Analysis Date = 11/11/15 Pct Recovery = 109% Analysis Date = 11/11/15 Pct Recovery = 109% Analysis Date = 11/06/15 Pct Recovery = 109% Analysis Date = 11/06/15 Pct Recovery = 109% Analysis Date = 11/01/15 Pct Recovery = 109% Analysis Date = 11/01/15 Pct Recovery = 109% Analysis Date = 10/27/15 Pct Recovery = 108% Analysis Date = 10/27/15 Pct Recovery = 108% Analysis Date = 10/23/15 Pct Recovery = 108% Analysis Date = 10/23/15 Pct Recovery = 108% Analysis Date = 10/18/15 Pct Recovery = 108% Analysis Date = 10/18/15 Pct Recovery = 108% Analysis Date = 10/13/15 Pct Recovery = 108% Analysis Date = 10/13/15 Pct Recovery = 108% Analysis Date = 10/08/15 Pct Recovery = 108% Analysis Date = 10/08/15 Pct Recovery = 108% Analysis Date = 10/04/15 Pct Recovery = 108% Analysis Date = 10/04/15 Pct Recovery = 108% Analysis Date = 09/29/15 Pct Recovery = 108% Analysis Date = 09/29/15 Pct Recovery = 108% Analysis Date = 09/24/15 Pct Recovery = 108% Analysis Date = 09/24/15 Pct Recovery = 108% Analysis Date = 09/19/15 Pct Recovery = 108% Analysis Date = 09/19/15 Pct Recovery = 108% Analysis Date = 09/14/15 Pct Recovery = 108% Analysis Date = 09/14/15 Pct Recovery = 108% Analysis Date = 09/10/15 Pct Recovery = 108% Analysis Date = 09/10/15 Pct Recovery = 108% Analysis Date = 09/05/15 Pct Recovery = 108% Analysis Date = 09/05/15 Pct Recovery = 108% Analysis Date = 08/31/15 Pct Recovery = 108% Analysis Date = 08/31/15 Pct Recovery = 108% Analysis Date = 08/26/15 Pct Recovery = 108% Analysis Date = 08/26/15 Pct Recovery = 108% Analysis Date = 08/21/15 Pct Recovery = 108% Analysis Date = 08/21/15 Pct Recovery = 108% Analysis Date = 08/17/15 Pct Recovery = 108% Analysis Date = 08/17/15 Pct Recovery = 108% Analysis Date = 08/12/15 Pct Recovery = 108% Analysis Date = 08/12/15 Pct Recovery = 108% Analysis Date = 08/07/15 Pct Recovery = 108% Analysis Date = 08/07/15 Pct Recovery = 108% Analysis Date = 08/02/15 Pct Recovery = 108% Analysis Date = 08/02/15 Pct Recovery = 108% Analysis Date = 07/29/15 Pct Recovery = 108% Analysis Date = 07/29/15 Pct Recovery = 108% Analysis Date = 07/24/15 Pct Recovery = 108% Analysis Date = 07/24/15 Pct Recovery = 108% Analysis Date = 07/19/15 Pct Recovery = 108% Analysis Date = 07/19/15 Pct Recovery = 108% Analysis Date = 07/14/15 Pct Recovery = 108% Analysis Date = 07/14/15 Pct Recovery = 108% Analysis Date = 07/09/15 Pct Recovery = 108% Analysis Date = 07/09/15 Pct Recovery = 108% Analysis Date = 07/05/15 Pct Recovery = 109% Analysis Date = 07/05/15 Pct Recovery = 109% Analysis Date = 06/30/15 Pct Recovery = 109% Analysis Date = 06/30/15 Pct Recovery = 109% Analysis Date = 06/25/15 Pct Recovery = 109% Analysis Date = 06/25/15 Pct Recovery = 109% Analysis Date = 06/20/15 Pct Recovery = 109% Analysis Date = 06/20/15 Pct Recovery = 109% Analysis Date = 06/16/15 Pct Recovery = 109% Analysis Date = 06/16/15 Pct Recovery = 109% Analysis Date = 06/11/15 Pct Recovery = 109% Analysis Date = 06/11/15 Pct Recovery = 109% Analysis Date = 06/06/15 Pct Recovery = 109% Analysis Date = 06/06/15 Pct Recovery = 109% Analysis Date = 06/01/15 Pct Recovery = 109% Analysis Date = 06/01/15 Pct Recovery = 109% Analysis Date = 05/27/15 Pct Recovery = 109% Analysis Date = 05/27/15 Pct Recovery = 109% Analysis Date = 05/23/15 Pct Recovery = 109% Analysis Date = 05/23/15 Pct Recovery = 109% Analysis Date = 05/18/15 Pct Recovery = 110% Analysis Date = 05/18/15 Pct Recovery = 110% Analysis Date = 05/13/15 Pct Recovery = 110% Analysis Date = 05/13/15 Pct Recovery = 110% Analysis Date = 05/08/15 Pct Recovery = 110% Analysis Date = 05/08/15 Pct Recovery = 110% Analysis Date = 05/04/15 Pct Recovery = 110% Analysis Date = 05/04/15 Pct Recovery = 110% Analysis Date = 04/29/15 Pct Recovery = 110% Analysis Date = 04/29/15 Pct Recovery = 110% Analysis Date = 04/24/15 Pct Recovery = 110% Analysis Date = 04/24/15 Pct Recovery = 110% Analysis Date = 04/19/15 Pct Recovery = 111% Analysis Date = 04/19/15 Pct Recovery = 111% Analysis Date = 04/14/15 Pct Recovery = 111% Analysis Date = 04/14/15 Pct Recovery = 111% Analysis Date = 04/10/15 Pct Recovery = 111% Analysis Date = 04/10/15 Pct Recovery = 111% Analysis Date = 04/05/15 Pct Recovery = 111% Analysis Date = 04/05/15 Pct Recovery = 111% Analysis Date = 03/31/15 Pct Recovery = 111% Analysis Date = 03/31/15 Pct Recovery = 111% Analysis Date = 03/26/15 Pct Recovery = 111% Analysis Date = 03/26/15 Pct Recovery = 111% Analysis Date = 03/22/15 Pct Recovery = 112% Analysis Date = 03/22/15 Pct Recovery = 112% Analysis Date = 03/17/15 Pct Recovery = 112% Analysis Date = 03/17/15 Pct Recovery = 112% Analysis Date = 03/12/15 Pct Recovery = 112% Analysis Date = 03/12/15 Pct Recovery = 112% Analysis Date = 03/07/15 Pct Recovery = 112% Analysis Date = 03/07/15 Pct Recovery = 112% Analysis Date = 03/02/15 Pct Recovery = 112% Analysis Date = 03/02/15 Pct Recovery = 112% Analysis Date = 02/26/15 Pct Recovery = 113% Analysis Date = 02/26/15 Pct Recovery = 113% Analysis Date = 02/21/15 Pct Recovery = 113% Analysis Date = 02/21/15 Pct Recovery = 113% Analysis Date = 02/16/15 Pct Recovery = 113% Analysis Date = 02/16/15 Pct Recovery = 113% Analysis Date = 02/11/15 Pct Recovery = 113% Analysis Date = 02/11/15 Pct Recovery = 113% Analysis Date = 02/07/15 Pct Recovery = 114% Analysis Date = 02/07/15 Pct Recovery = 114% Analysis Date = 02/02/15 Pct Recovery = 114% Analysis Date = 02/02/15 Pct Recovery = 114% Analysis Date = 01/28/15 Pct Recovery = 114% Analysis Date = 01/28/15 Pct Recovery = 114% Analysis Date = 01/23/15 Pct Recovery = 114% Analysis Date = 01/23/15 Pct Recovery = 114% Analysis Date = 01/18/15 Pct Recovery = 115% Analysis Date = 01/18/15 Pct Recovery = 115% Analysis Date = 01/14/15 Pct Recovery = 115% Analysis Date = 01/14/15 Pct Recovery = 115% Analysis Date = 01/09/15 Pct Recovery = 115% Analysis Date = 01/09/15 Pct Recovery = 115% Analysis Date = 01/04/15 Pct Recovery = 115% Analysis Date = 01/04/15 Pct Recovery = 115% Analysis Date = 12/30/14 Pct Recovery = 116% Analysis Date = 12/30/14 Pct Recovery = 116% Analysis Date = 12/25/14 Pct Recovery = 116% Analysis Date = 12/25/14 Pct Recovery = 116% Analysis Date = 12/21/14 Pct Recovery = 116% Analysis Date = 12/21/14 Pct Recovery = 116% Analysis Date = 12/16/14 Pct Recovery = 116% Analysis Date = 12/16/14 Pct Recovery = 116% Analysis Date = 12/11/14 Pct Recovery = 117% Analysis Date = 12/11/14 Pct Recovery = 117% Analysis Date = 12/06/14 Pct Recovery = 117% Analysis Date = 12/06/14 Pct Recovery = 117% Analysis Date = 12/02/14 Pct Recovery = 117% Analysis Date = 12/02/14 Pct Recovery = 117% Analysis Date = 11/27/14 Pct Recovery = 117% Analysis Date = 11/27/14 Pct Recovery = 117% Analysis Date = 11/22/14 Pct Recovery = 118% Analysis Date = 11/22/14 Pct Recovery = 118% Analysis Date = 11/17/14 Pct Recovery = 118% Analysis Date = 11/17/14 Pct Recovery = 118% Analysis Date = 11/12/14 Pct Recovery = 118% Analysis Date = 11/12/14 Pct Recovery = 118% Analysis Date = 11/08/14 Pct Recovery = 118% Analysis Date = 11/08/14 Pct Recovery = 118% Analysis Date = 11/03/14 Pct Recovery = 119% Analysis Date = 11/03/14 Pct Recovery = 119% Analysis Date = 10/29/14 Pct Recovery = 119% Analysis Date = 10/29/14 Pct Recovery = 119% Analysis Date = 10/24/14 Pct Recovery = 119% Analysis Date = 10/24/14 Pct Recovery = 119% Analysis Date = 10/20/14 Pct Recovery = 119% Analysis Date = 10/20/14 Pct Recovery = 119% Analysis Date = 10/15/14 Pct Recovery = 120% Analysis Date = 10/15/14 Pct Recovery = 120% Analysis Date = 10/10/14 Pct Recovery = 120% Analysis Date = 10/10/14 Pct Recovery = 120% Analysis Date = 10/05/14 Pct Recovery = 120% Analysis Date = 10/05/14 Pct Recovery = 120% Analysis Date = 09/30/14 Pct Recovery = 120% Analysis Date = 09/30/14 Pct Recovery = 120% Analysis Date = 09/26/14 Pct Recovery = 121% Analysis Date = 09/26/14 Pct Recovery = 121% Analysis Date = 09/21/14 Pct Recovery = 121% Analysis Date = 09/21/14 Pct Recovery = 121% Analysis Date = 09/16/14 Pct Recovery = 121% Analysis Date = 09/16/14 Pct Recovery = 121% Analysis Date = 09/11/14 Pct Recovery = 121% Analysis Date = 09/11/14 Pct Recovery = 121% Analysis Date = 09/07/14 Pct Recovery = 122% Analysis Date = 09/07/14 Pct Recovery = 122% Analysis Date = 09/02/14 Pct Recovery = 122% Analysis Date = 09/02/14 Pct Recovery = 122% Analysis Date = 08/28/14 Pct Recovery = 122% Analysis Date = 08/28/14 Pct Recovery = 122% Analysis Date = 08/23/14 Pct Recovery = 123% Analysis Date = 08/23/14 Pct Recovery = 123% Analysis Date = 08/18/14 Pct Recovery = 123% Analysis Date = 08/18/14 Pct Recovery = 123% Analysis Date = 08/14/14 Pct Recovery = 123% Analysis Date = 08/14/14 Pct Recovery = 123% Analysis Date = 08/09/14 Pct Recovery = 123% Analysis Date = 08/09/14 Pct Recovery = 123% Analysis Date = 08/04/14 Pct Recovery = 124% Analysis Date = 08/04/14 Pct Recovery = 124% Analysis Date = 07/30/14 Pct Recovery = 124% Analysis Date = 07/30/14 Pct Recovery = 124% Analysis Date = 07/26/14 Pct Recovery = 124% Analysis Date = 07/26/14 Pct Recovery = 124% Analysis Date = 07/21/14 Pct Recovery = 124% Analysis Date = 07/21/14 Pct Recovery = 124% Analysis Date = 07/16/14 Pct Recovery = 125% Analysis Date = 07/16/14 Pct Recovery = 125% Analysis Date = 07/11/14 Pct Recovery = 125% Analysis Date = 07/11/14 Pct Recovery = 125% Analysis Date = 07/06/14 Pct Recovery = 125% Analysis Date = 07/06/14 Pct Recovery = 125% Analysis Date = 07/02/14 Pct Recovery = 126% Analysis Date = 07/02/14 Pct Recovery = 126% Analysis Date = 06/27/14 Pct Recovery = 126% Analysis Date = 06/27/14 Pct Recovery = 126% Analysis Date = 06/22/14 Pct Recovery = 126% Analysis Date = 06/22/14 Pct Recovery = 126% Analysis Date = 06/17/14 Pct Recovery = 126% Analysis Date = 06/17/14 Pct Recovery = 126% Analysis Date = 06/13/14 Pct Recovery = 127% Analysis Date = 06/13/14 Pct Recovery = 127% Analysis Date = 06/08/14 Pct Recovery = 127% Analysis Date = 06/08/14 Pct Recovery = 127% Analysis Date = 06/03/14 Pct Recovery = 127% Analysis Date = 06/03/14 Pct Recovery = 127% Analysis Date = 05/29/14 Pct Recovery = 128% Analysis Date = 05/29/14 Pct Recovery = 128% Analysis Date = 05/24/14 Pct Recovery = 128% Analysis Date = 05/24/14 Pct Recovery = 128% Analysis Date = 05/20/14 Pct Recovery = 128% Analysis Date = 05/20/14 Pct Recovery = 128% Analysis Date = 05/15/14 Pct Recovery = 128% Analysis Date = 05/15/14 Pct Recovery = 128% Analysis Date = 05/10/14 Pct Recovery = 129% Analysis Date = 05/10/14 Pct Recovery = 129% Analysis Date = 05/05/14 Pct Recovery = 129% Analysis Date = 05/05/14 Pct Recovery = 129% Analysis Date = 05/01/14 Pct Recovery = 129% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
ACETONE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 47 113% 16% 114% 12%
Total 47 113% 16% 114% 12%

Sample Statistics
ACETONE

Characteristic N % % Basis
Plotted 47 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 47 .  
False Negatives 0 0% 0 out of 47
Not Spiked 26 .  
False Positives 1 4% 1 out of 26

BQS OBSP Determination:
ACRYLONITRILE
METHOD: 4440 , TESTIDCODE: 34215GCM66
Open Data Set

Analysis Date = 12/12/16 SpikeMix = Accu 216041125: 40 µl & Crescent 03FF058: 40 µl Pct Recovery = 106% Analysis Date = 07/20/16 SpikeMix = Supelco LC20141V: 40 µl & Accu 216041125: 40 µl Pct Recovery = 106% Analysis Date = 07/14/16 SpikeMix = Accu 216041125: 40 µl & NSI 041816AVOC: 40 µl Pct Recovery = 91% Analysis Date = 09/08/16 SpikeMix = Supelco LC20141V: 25 µl & Accu 216041125: 25 µl Pct Recovery = 101% Analysis Date = 05/24/16 SpikeMix = Accu 216041125: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 94% Analysis Date = 08/12/16 SpikeMix = ChemService 5082900: 25 µl & Phenova B20160319: 25 µl Pct Recovery = 98% Analysis Date = 06/21/16 SpikeMix = Phenova B20160319: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 109% Analysis Date = 04/09/15 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 95% Analysis Date = 03/06/15 SpikeMix = ERA 0227-14-06.1A: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 122% Analysis Date = 11/22/14 SpikeMix = NSI 032614: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 98% Analysis Date = 11/14/14 SpikeMix = Crescent 03DD004: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 105% Analysis Date = 08/16/14 SpikeMix = ERA 0227-14-06.1A: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 109% Analysis Date = 07/01/14 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 109% Analysis Date = 06/10/14 SpikeMix = Crescent 03DD004: 20 µl & NSI 032614: 20 µl Pct Recovery = 94% Analysis Date = 06/10/14 SpikeMix = NSI 032614: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 112% Analysis Date = 05/01/14 SpikeMix = Accu 214031115: 20 µl & NSI 032614: 20 µl Pct Recovery = 95% Analysis Date = 08/15/15 SpikeMix = Supelco LC13545: 25 µl & Crescent 04EE008: 25 µl Pct Recovery = 94% Analysis Date = 06/16/15 SpikeMix = ERA 0406-15-03: 25 µl & Supelco LC13545: 25 µl Pct Recovery = 83% Analysis Date = 10/13/16 SpikeMix = Accu 216041125: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 102% Analysis Date = 08/20/16 SpikeMix = Accu 216041125: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 116% Analysis Date = 06/30/16 SpikeMix = ChemService 5082900: 15 µl & Accu 216041125: 15 µl Pct Recovery = 76% Analysis Date = 11/29/16 SpikeMix = ChemService 5082900: 15 µl & Phenova B20160319: 15 µl Pct Recovery = 103% Analysis Date = 09/08/16 SpikeMix = Phenova B20160319: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 100% Analysis Date = 07/29/16 SpikeMix = Phenova B20160319: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 89% Analysis Date = 05/27/16 SpikeMix = Phenova B20160319: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 98% Analysis Date = 04/26/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 113% Analysis Date = 02/05/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 93% Analysis Date = 11/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 119% Analysis Date = 10/16/15 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 104% Analysis Date = 05/09/15 SpikeMix = Spex Organics EN150428007: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 111% Analysis Date = 04/02/16 SpikeMix = Supelco LC13545: 15 µl & Accu 215041380: 15 µl Pct Recovery = 99% Analysis Date = 12/18/15 SpikeMix = Supelco LC13545: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 113% Analysis Date = 01/13/15 SpikeMix = Accu 214031115: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 107% Analysis Date = 10/21/14 SpikeMix = ERA 0227-14-06.1A: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 102% Analysis Date = 10/04/14 SpikeMix = Crescent 03DD004: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 105% Analysis Date = 09/09/14 SpikeMix = Accu 214031115: 10 µl & NSI 032614: 10 µl Pct Recovery = 115% Analysis Date = 09/09/14 SpikeMix = NSI 032614: 10 µl & Spex Organics C1140417015: 10 µl Pct Recovery = 117% Analysis Date = 07/29/14 SpikeMix = Crescent 03DD004: 10 µl & NSI 032614: 10 µl Pct Recovery = 98% Analysis Date = 07/11/14 SpikeMix = Spex Organics C1140417015: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 113% Analysis Date = 05/30/14 SpikeMix = NSI 032614: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 105% Analysis Date = 02/18/16 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 104% Analysis Date = 11/12/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 118% Analysis Date = 09/03/15 SpikeMix = NSI 050515AVOC: 10 µl & Spex Organics EN150428007: 10 µl Pct Recovery = 83% Analysis Date = 05/21/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 123% Analysis Date = 05/13/16 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 97% Analysis Date = 03/17/16 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 100% Analysis Date = 12/10/15 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 94% Analysis Date = 06/27/15 SpikeMix = ERA 0406-15-03: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 114% Analysis Date = 05/09/15 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 105% Analysis Date = 12/11/16 Pct Recovery = 100% Analysis Date = 12/07/16 Pct Recovery = 100% Analysis Date = 12/07/16 Pct Recovery = 100% Analysis Date = 12/02/16 Pct Recovery = 100% Analysis Date = 12/02/16 Pct Recovery = 100% Analysis Date = 11/27/16 Pct Recovery = 100% Analysis Date = 11/27/16 Pct Recovery = 100% Analysis Date = 11/22/16 Pct Recovery = 100% Analysis Date = 11/22/16 Pct Recovery = 100% Analysis Date = 11/18/16 Pct Recovery = 100% Analysis Date = 11/18/16 Pct Recovery = 100% Analysis Date = 11/13/16 Pct Recovery = 100% Analysis Date = 11/13/16 Pct Recovery = 100% Analysis Date = 11/08/16 Pct Recovery = 100% Analysis Date = 11/08/16 Pct Recovery = 100% Analysis Date = 11/03/16 Pct Recovery = 100% Analysis Date = 11/03/16 Pct Recovery = 100% Analysis Date = 10/29/16 Pct Recovery = 100% Analysis Date = 10/29/16 Pct Recovery = 100% Analysis Date = 10/25/16 Pct Recovery = 100% Analysis Date = 10/25/16 Pct Recovery = 100% Analysis Date = 10/20/16 Pct Recovery = 100% Analysis Date = 10/20/16 Pct Recovery = 100% Analysis Date = 10/15/16 Pct Recovery = 100% Analysis Date = 10/15/16 Pct Recovery = 100% Analysis Date = 10/10/16 Pct Recovery = 100% Analysis Date = 10/10/16 Pct Recovery = 100% Analysis Date = 10/06/16 Pct Recovery = 100% Analysis Date = 10/06/16 Pct Recovery = 100% Analysis Date = 10/01/16 Pct Recovery = 100% Analysis Date = 10/01/16 Pct Recovery = 100% Analysis Date = 09/26/16 Pct Recovery = 100% Analysis Date = 09/26/16 Pct Recovery = 100% Analysis Date = 09/21/16 Pct Recovery = 100% Analysis Date = 09/21/16 Pct Recovery = 100% Analysis Date = 09/16/16 Pct Recovery = 100% Analysis Date = 09/16/16 Pct Recovery = 100% Analysis Date = 09/12/16 Pct Recovery = 100% Analysis Date = 09/12/16 Pct Recovery = 100% Analysis Date = 09/07/16 Pct Recovery = 100% Analysis Date = 09/07/16 Pct Recovery = 100% Analysis Date = 09/02/16 Pct Recovery = 100% Analysis Date = 09/02/16 Pct Recovery = 100% Analysis Date = 08/28/16 Pct Recovery = 100% Analysis Date = 08/28/16 Pct Recovery = 100% Analysis Date = 08/24/16 Pct Recovery = 100% Analysis Date = 08/24/16 Pct Recovery = 100% Analysis Date = 08/19/16 Pct Recovery = 100% Analysis Date = 08/19/16 Pct Recovery = 100% Analysis Date = 08/14/16 Pct Recovery = 100% Analysis Date = 08/14/16 Pct Recovery = 100% Analysis Date = 08/09/16 Pct Recovery = 100% Analysis Date = 08/09/16 Pct Recovery = 100% Analysis Date = 08/04/16 Pct Recovery = 100% Analysis Date = 08/04/16 Pct Recovery = 100% Analysis Date = 07/31/16 Pct Recovery = 100% Analysis Date = 07/31/16 Pct Recovery = 100% Analysis Date = 07/26/16 Pct Recovery = 100% Analysis Date = 07/26/16 Pct Recovery = 100% Analysis Date = 07/21/16 Pct Recovery = 100% Analysis Date = 07/21/16 Pct Recovery = 100% Analysis Date = 07/16/16 Pct Recovery = 100% Analysis Date = 07/16/16 Pct Recovery = 100% Analysis Date = 07/12/16 Pct Recovery = 100% Analysis Date = 07/12/16 Pct Recovery = 100% Analysis Date = 07/07/16 Pct Recovery = 100% Analysis Date = 07/07/16 Pct Recovery = 100% Analysis Date = 07/02/16 Pct Recovery = 100% Analysis Date = 07/02/16 Pct Recovery = 100% Analysis Date = 06/27/16 Pct Recovery = 100% Analysis Date = 06/27/16 Pct Recovery = 100% Analysis Date = 06/22/16 Pct Recovery = 100% Analysis Date = 06/22/16 Pct Recovery = 100% Analysis Date = 06/18/16 Pct Recovery = 101% Analysis Date = 06/18/16 Pct Recovery = 101% Analysis Date = 06/13/16 Pct Recovery = 101% Analysis Date = 06/13/16 Pct Recovery = 101% Analysis Date = 06/08/16 Pct Recovery = 101% Analysis Date = 06/08/16 Pct Recovery = 101% Analysis Date = 06/03/16 Pct Recovery = 101% Analysis Date = 06/03/16 Pct Recovery = 101% Analysis Date = 05/30/16 Pct Recovery = 101% Analysis Date = 05/30/16 Pct Recovery = 101% Analysis Date = 05/25/16 Pct Recovery = 101% Analysis Date = 05/25/16 Pct Recovery = 101% Analysis Date = 05/20/16 Pct Recovery = 101% Analysis Date = 05/20/16 Pct Recovery = 101% Analysis Date = 05/15/16 Pct Recovery = 101% Analysis Date = 05/15/16 Pct Recovery = 101% Analysis Date = 05/10/16 Pct Recovery = 101% Analysis Date = 05/10/16 Pct Recovery = 101% Analysis Date = 05/06/16 Pct Recovery = 101% Analysis Date = 05/06/16 Pct Recovery = 101% Analysis Date = 05/01/16 Pct Recovery = 101% Analysis Date = 05/01/16 Pct Recovery = 101% Analysis Date = 04/26/16 Pct Recovery = 101% Analysis Date = 04/26/16 Pct Recovery = 101% Analysis Date = 04/21/16 Pct Recovery = 101% Analysis Date = 04/21/16 Pct Recovery = 101% Analysis Date = 04/16/16 Pct Recovery = 101% Analysis Date = 04/16/16 Pct Recovery = 101% Analysis Date = 04/12/16 Pct Recovery = 101% Analysis Date = 04/12/16 Pct Recovery = 101% Analysis Date = 04/07/16 Pct Recovery = 101% Analysis Date = 04/07/16 Pct Recovery = 101% Analysis Date = 04/02/16 Pct Recovery = 101% Analysis Date = 04/02/16 Pct Recovery = 101% Analysis Date = 03/28/16 Pct Recovery = 101% Analysis Date = 03/28/16 Pct Recovery = 101% Analysis Date = 03/24/16 Pct Recovery = 101% Analysis Date = 03/24/16 Pct Recovery = 101% Analysis Date = 03/19/16 Pct Recovery = 101% Analysis Date = 03/19/16 Pct Recovery = 101% Analysis Date = 03/14/16 Pct Recovery = 101% Analysis Date = 03/14/16 Pct Recovery = 101% Analysis Date = 03/09/16 Pct Recovery = 101% Analysis Date = 03/09/16 Pct Recovery = 101% Analysis Date = 03/04/16 Pct Recovery = 102% Analysis Date = 03/04/16 Pct Recovery = 102% Analysis Date = 02/29/16 Pct Recovery = 102% Analysis Date = 02/29/16 Pct Recovery = 102% Analysis Date = 02/24/16 Pct Recovery = 102% Analysis Date = 02/24/16 Pct Recovery = 102% Analysis Date = 02/19/16 Pct Recovery = 102% Analysis Date = 02/19/16 Pct Recovery = 102% Analysis Date = 02/14/16 Pct Recovery = 102% Analysis Date = 02/14/16 Pct Recovery = 102% Analysis Date = 02/10/16 Pct Recovery = 102% Analysis Date = 02/10/16 Pct Recovery = 102% Analysis Date = 02/05/16 Pct Recovery = 102% Analysis Date = 02/05/16 Pct Recovery = 102% Analysis Date = 01/31/16 Pct Recovery = 102% Analysis Date = 01/31/16 Pct Recovery = 102% Analysis Date = 01/26/16 Pct Recovery = 102% Analysis Date = 01/26/16 Pct Recovery = 102% Analysis Date = 01/21/16 Pct Recovery = 102% Analysis Date = 01/21/16 Pct Recovery = 102% Analysis Date = 01/17/16 Pct Recovery = 102% Analysis Date = 01/17/16 Pct Recovery = 102% Analysis Date = 01/12/16 Pct Recovery = 102% Analysis Date = 01/12/16 Pct Recovery = 102% Analysis Date = 01/07/16 Pct Recovery = 102% Analysis Date = 01/07/16 Pct Recovery = 102% Analysis Date = 01/02/16 Pct Recovery = 102% Analysis Date = 01/02/16 Pct Recovery = 102% Analysis Date = 12/29/15 Pct Recovery = 102% Analysis Date = 12/29/15 Pct Recovery = 102% Analysis Date = 12/24/15 Pct Recovery = 102% Analysis Date = 12/24/15 Pct Recovery = 102% Analysis Date = 12/19/15 Pct Recovery = 102% Analysis Date = 12/19/15 Pct Recovery = 102% Analysis Date = 12/14/15 Pct Recovery = 102% Analysis Date = 12/14/15 Pct Recovery = 102% Analysis Date = 12/09/15 Pct Recovery = 102% Analysis Date = 12/09/15 Pct Recovery = 102% Analysis Date = 12/05/15 Pct Recovery = 102% Analysis Date = 12/05/15 Pct Recovery = 102% Analysis Date = 11/30/15 Pct Recovery = 103% Analysis Date = 11/30/15 Pct Recovery = 103% Analysis Date = 11/25/15 Pct Recovery = 103% Analysis Date = 11/25/15 Pct Recovery = 103% Analysis Date = 11/20/15 Pct Recovery = 103% Analysis Date = 11/20/15 Pct Recovery = 103% Analysis Date = 11/16/15 Pct Recovery = 103% Analysis Date = 11/16/15 Pct Recovery = 103% Analysis Date = 11/11/15 Pct Recovery = 103% Analysis Date = 11/11/15 Pct Recovery = 103% Analysis Date = 11/06/15 Pct Recovery = 103% Analysis Date = 11/06/15 Pct Recovery = 103% Analysis Date = 11/01/15 Pct Recovery = 103% Analysis Date = 11/01/15 Pct Recovery = 103% Analysis Date = 10/27/15 Pct Recovery = 103% Analysis Date = 10/27/15 Pct Recovery = 103% Analysis Date = 10/23/15 Pct Recovery = 103% Analysis Date = 10/23/15 Pct Recovery = 103% Analysis Date = 10/18/15 Pct Recovery = 103% Analysis Date = 10/18/15 Pct Recovery = 103% Analysis Date = 10/13/15 Pct Recovery = 103% Analysis Date = 10/13/15 Pct Recovery = 103% Analysis Date = 10/08/15 Pct Recovery = 103% Analysis Date = 10/08/15 Pct Recovery = 103% Analysis Date = 10/04/15 Pct Recovery = 103% Analysis Date = 10/04/15 Pct Recovery = 103% Analysis Date = 09/29/15 Pct Recovery = 104% Analysis Date = 09/29/15 Pct Recovery = 104% Analysis Date = 09/24/15 Pct Recovery = 104% Analysis Date = 09/24/15 Pct Recovery = 104% Analysis Date = 09/19/15 Pct Recovery = 104% Analysis Date = 09/19/15 Pct Recovery = 104% Analysis Date = 09/14/15 Pct Recovery = 104% Analysis Date = 09/14/15 Pct Recovery = 104% Analysis Date = 09/10/15 Pct Recovery = 104% Analysis Date = 09/10/15 Pct Recovery = 104% Analysis Date = 09/05/15 Pct Recovery = 104% Analysis Date = 09/05/15 Pct Recovery = 104% Analysis Date = 08/31/15 Pct Recovery = 104% Analysis Date = 08/31/15 Pct Recovery = 104% Analysis Date = 08/26/15 Pct Recovery = 104% Analysis Date = 08/26/15 Pct Recovery = 104% Analysis Date = 08/21/15 Pct Recovery = 104% Analysis Date = 08/21/15 Pct Recovery = 104% Analysis Date = 08/17/15 Pct Recovery = 104% Analysis Date = 08/17/15 Pct Recovery = 104% Analysis Date = 08/12/15 Pct Recovery = 104% Analysis Date = 08/12/15 Pct Recovery = 104% Analysis Date = 08/07/15 Pct Recovery = 104% Analysis Date = 08/07/15 Pct Recovery = 104% Analysis Date = 08/02/15 Pct Recovery = 104% Analysis Date = 08/02/15 Pct Recovery = 104% Analysis Date = 07/29/15 Pct Recovery = 104% Analysis Date = 07/29/15 Pct Recovery = 104% Analysis Date = 07/24/15 Pct Recovery = 104% Analysis Date = 07/24/15 Pct Recovery = 104% Analysis Date = 07/19/15 Pct Recovery = 105% Analysis Date = 07/19/15 Pct Recovery = 105% Analysis Date = 07/14/15 Pct Recovery = 105% Analysis Date = 07/14/15 Pct Recovery = 105% Analysis Date = 07/09/15 Pct Recovery = 105% Analysis Date = 07/09/15 Pct Recovery = 105% Analysis Date = 07/05/15 Pct Recovery = 105% Analysis Date = 07/05/15 Pct Recovery = 105% Analysis Date = 06/30/15 Pct Recovery = 105% Analysis Date = 06/30/15 Pct Recovery = 105% Analysis Date = 06/25/15 Pct Recovery = 105% Analysis Date = 06/25/15 Pct Recovery = 105% Analysis Date = 06/20/15 Pct Recovery = 105% Analysis Date = 06/20/15 Pct Recovery = 105% Analysis Date = 06/16/15 Pct Recovery = 105% Analysis Date = 06/16/15 Pct Recovery = 105% Analysis Date = 06/11/15 Pct Recovery = 105% Analysis Date = 06/11/15 Pct Recovery = 105% Analysis Date = 06/06/15 Pct Recovery = 105% Analysis Date = 06/06/15 Pct Recovery = 105% Analysis Date = 06/01/15 Pct Recovery = 105% Analysis Date = 06/01/15 Pct Recovery = 105% Analysis Date = 05/27/15 Pct Recovery = 105% Analysis Date = 05/27/15 Pct Recovery = 105% Analysis Date = 05/23/15 Pct Recovery = 105% Analysis Date = 05/23/15 Pct Recovery = 105% Analysis Date = 05/18/15 Pct Recovery = 105% Analysis Date = 05/18/15 Pct Recovery = 105% Analysis Date = 05/13/15 Pct Recovery = 105% Analysis Date = 05/13/15 Pct Recovery = 105% Analysis Date = 05/08/15 Pct Recovery = 105% Analysis Date = 05/08/15 Pct Recovery = 105% Analysis Date = 05/04/15 Pct Recovery = 105% Analysis Date = 05/04/15 Pct Recovery = 105% Analysis Date = 04/29/15 Pct Recovery = 105% Analysis Date = 04/29/15 Pct Recovery = 105% Analysis Date = 04/24/15 Pct Recovery = 105% Analysis Date = 04/24/15 Pct Recovery = 105% Analysis Date = 04/19/15 Pct Recovery = 105% Analysis Date = 04/19/15 Pct Recovery = 105% Analysis Date = 04/14/15 Pct Recovery = 105% Analysis Date = 04/14/15 Pct Recovery = 105% Analysis Date = 04/10/15 Pct Recovery = 105% Analysis Date = 04/10/15 Pct Recovery = 105% Analysis Date = 04/05/15 Pct Recovery = 105% Analysis Date = 04/05/15 Pct Recovery = 105% Analysis Date = 03/31/15 Pct Recovery = 105% Analysis Date = 03/31/15 Pct Recovery = 105% Analysis Date = 03/26/15 Pct Recovery = 105% Analysis Date = 03/26/15 Pct Recovery = 105% Analysis Date = 03/22/15 Pct Recovery = 105% Analysis Date = 03/22/15 Pct Recovery = 105% Analysis Date = 03/17/15 Pct Recovery = 105% Analysis Date = 03/17/15 Pct Recovery = 105% Analysis Date = 03/12/15 Pct Recovery = 105% Analysis Date = 03/12/15 Pct Recovery = 105% Analysis Date = 03/07/15 Pct Recovery = 105% Analysis Date = 03/07/15 Pct Recovery = 105% Analysis Date = 03/02/15 Pct Recovery = 105% Analysis Date = 03/02/15 Pct Recovery = 105% Analysis Date = 02/26/15 Pct Recovery = 105% Analysis Date = 02/26/15 Pct Recovery = 105% Analysis Date = 02/21/15 Pct Recovery = 105% Analysis Date = 02/21/15 Pct Recovery = 105% Analysis Date = 02/16/15 Pct Recovery = 105% Analysis Date = 02/16/15 Pct Recovery = 105% Analysis Date = 02/11/15 Pct Recovery = 106% Analysis Date = 02/11/15 Pct Recovery = 106% Analysis Date = 02/07/15 Pct Recovery = 106% Analysis Date = 02/07/15 Pct Recovery = 106% Analysis Date = 02/02/15 Pct Recovery = 106% Analysis Date = 02/02/15 Pct Recovery = 106% Analysis Date = 01/28/15 Pct Recovery = 106% Analysis Date = 01/28/15 Pct Recovery = 106% Analysis Date = 01/23/15 Pct Recovery = 106% Analysis Date = 01/23/15 Pct Recovery = 106% Analysis Date = 01/18/15 Pct Recovery = 106% Analysis Date = 01/18/15 Pct Recovery = 106% Analysis Date = 01/14/15 Pct Recovery = 106% Analysis Date = 01/14/15 Pct Recovery = 106% Analysis Date = 01/09/15 Pct Recovery = 106% Analysis Date = 01/09/15 Pct Recovery = 106% Analysis Date = 01/04/15 Pct Recovery = 106% Analysis Date = 01/04/15 Pct Recovery = 106% Analysis Date = 12/30/14 Pct Recovery = 106% Analysis Date = 12/30/14 Pct Recovery = 106% Analysis Date = 12/25/14 Pct Recovery = 106% Analysis Date = 12/25/14 Pct Recovery = 106% Analysis Date = 12/21/14 Pct Recovery = 106% Analysis Date = 12/21/14 Pct Recovery = 106% Analysis Date = 12/16/14 Pct Recovery = 106% Analysis Date = 12/16/14 Pct Recovery = 106% Analysis Date = 12/11/14 Pct Recovery = 106% Analysis Date = 12/11/14 Pct Recovery = 106% Analysis Date = 12/06/14 Pct Recovery = 106% Analysis Date = 12/06/14 Pct Recovery = 106% Analysis Date = 12/02/14 Pct Recovery = 106% Analysis Date = 12/02/14 Pct Recovery = 106% Analysis Date = 11/27/14 Pct Recovery = 106% Analysis Date = 11/27/14 Pct Recovery = 106% Analysis Date = 11/22/14 Pct Recovery = 106% Analysis Date = 11/22/14 Pct Recovery = 106% Analysis Date = 11/17/14 Pct Recovery = 106% Analysis Date = 11/17/14 Pct Recovery = 106% Analysis Date = 11/12/14 Pct Recovery = 106% Analysis Date = 11/12/14 Pct Recovery = 106% Analysis Date = 11/08/14 Pct Recovery = 106% Analysis Date = 11/08/14 Pct Recovery = 106% Analysis Date = 11/03/14 Pct Recovery = 106% Analysis Date = 11/03/14 Pct Recovery = 106% Analysis Date = 10/29/14 Pct Recovery = 106% Analysis Date = 10/29/14 Pct Recovery = 106% Analysis Date = 10/24/14 Pct Recovery = 106% Analysis Date = 10/24/14 Pct Recovery = 106% Analysis Date = 10/20/14 Pct Recovery = 106% Analysis Date = 10/20/14 Pct Recovery = 106% Analysis Date = 10/15/14 Pct Recovery = 106% Analysis Date = 10/15/14 Pct Recovery = 106% Analysis Date = 10/10/14 Pct Recovery = 106% Analysis Date = 10/10/14 Pct Recovery = 106% Analysis Date = 10/05/14 Pct Recovery = 106% Analysis Date = 10/05/14 Pct Recovery = 106% Analysis Date = 09/30/14 Pct Recovery = 106% Analysis Date = 09/30/14 Pct Recovery = 106% Analysis Date = 09/26/14 Pct Recovery = 106% Analysis Date = 09/26/14 Pct Recovery = 106% Analysis Date = 09/21/14 Pct Recovery = 106% Analysis Date = 09/21/14 Pct Recovery = 106% Analysis Date = 09/16/14 Pct Recovery = 106% Analysis Date = 09/16/14 Pct Recovery = 106% Analysis Date = 09/11/14 Pct Recovery = 106% Analysis Date = 09/11/14 Pct Recovery = 106% Analysis Date = 09/07/14 Pct Recovery = 106% Analysis Date = 09/07/14 Pct Recovery = 106% Analysis Date = 09/02/14 Pct Recovery = 106% Analysis Date = 09/02/14 Pct Recovery = 106% Analysis Date = 08/28/14 Pct Recovery = 106% Analysis Date = 08/28/14 Pct Recovery = 106% Analysis Date = 08/23/14 Pct Recovery = 106% Analysis Date = 08/23/14 Pct Recovery = 106% Analysis Date = 08/18/14 Pct Recovery = 106% Analysis Date = 08/18/14 Pct Recovery = 106% Analysis Date = 08/14/14 Pct Recovery = 106% Analysis Date = 08/14/14 Pct Recovery = 106% Analysis Date = 08/09/14 Pct Recovery = 106% Analysis Date = 08/09/14 Pct Recovery = 106% Analysis Date = 08/04/14 Pct Recovery = 106% Analysis Date = 08/04/14 Pct Recovery = 106% Analysis Date = 07/30/14 Pct Recovery = 106% Analysis Date = 07/30/14 Pct Recovery = 106% Analysis Date = 07/26/14 Pct Recovery = 106% Analysis Date = 07/26/14 Pct Recovery = 106% Analysis Date = 07/21/14 Pct Recovery = 106% Analysis Date = 07/21/14 Pct Recovery = 106% Analysis Date = 07/16/14 Pct Recovery = 106% Analysis Date = 07/16/14 Pct Recovery = 106% Analysis Date = 07/11/14 Pct Recovery = 106% Analysis Date = 07/11/14 Pct Recovery = 106% Analysis Date = 07/06/14 Pct Recovery = 106% Analysis Date = 07/06/14 Pct Recovery = 106% Analysis Date = 07/02/14 Pct Recovery = 106% Analysis Date = 07/02/14 Pct Recovery = 106% Analysis Date = 06/27/14 Pct Recovery = 106% Analysis Date = 06/27/14 Pct Recovery = 106% Analysis Date = 06/22/14 Pct Recovery = 106% Analysis Date = 06/22/14 Pct Recovery = 106% Analysis Date = 06/17/14 Pct Recovery = 106% Analysis Date = 06/17/14 Pct Recovery = 106% Analysis Date = 06/13/14 Pct Recovery = 105% Analysis Date = 06/13/14 Pct Recovery = 105% Analysis Date = 06/08/14 Pct Recovery = 105% Analysis Date = 06/08/14 Pct Recovery = 105% Analysis Date = 06/03/14 Pct Recovery = 105% Analysis Date = 06/03/14 Pct Recovery = 105% Analysis Date = 05/29/14 Pct Recovery = 105% Analysis Date = 05/29/14 Pct Recovery = 105% Analysis Date = 05/24/14 Pct Recovery = 105% Analysis Date = 05/24/14 Pct Recovery = 105% Analysis Date = 05/20/14 Pct Recovery = 105% Analysis Date = 05/20/14 Pct Recovery = 105% Analysis Date = 05/15/14 Pct Recovery = 105% Analysis Date = 05/15/14 Pct Recovery = 105% Analysis Date = 05/10/14 Pct Recovery = 105% Analysis Date = 05/10/14 Pct Recovery = 105% Analysis Date = 05/05/14 Pct Recovery = 105% Analysis Date = 05/05/14 Pct Recovery = 105% Analysis Date = 05/01/14 Pct Recovery = 105% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
ACRYLONITRILE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 49 103% 10% 104% 10%
Total 49 103% 10% 104% 10%

Sample Statistics
ACRYLONITRILE

Characteristic N % % Basis
Plotted 49 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 49 .  
False Negatives 0 0% 0 out of 49
Not Spiked 24 .  
False Positives 0 0% 0 out of 24

BQS OBSP Determination:
BENZENE
METHOD: 4440 , TESTIDCODE: 34030GCM66
Open Data Set

Analysis Date = 12/16/16 SpikeMix = NSI 041816AVOC: 40 µl & ChemService 5082900: 40 µl Pct Recovery = 117% Analysis Date = 08/04/16 SpikeMix = Crescent 03FF058: 40 µl & Supelco LC20141V: 40 µl Pct Recovery = 93% Analysis Date = 07/20/16 SpikeMix = Supelco LC20141V: 40 µl & Accu 216041125: 40 µl Pct Recovery = 90% Analysis Date = 04/09/15 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 98% Analysis Date = 08/19/14 SpikeMix = Spex Organics C1140417015: 20 µl & Accu 214031115: 20 µl Pct Recovery = 102% Analysis Date = 07/01/14 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 103% Analysis Date = 05/01/14 SpikeMix = Accu 214031115: 20 µl & NSI 032614: 20 µl Pct Recovery = 102% Analysis Date = 11/21/16 SpikeMix = Crescent 03FF058: 25 µl & Supelco LC20141V: 25 µl Pct Recovery = 87% Analysis Date = 09/08/16 SpikeMix = Supelco LC20141V: 25 µl & Accu 216041125: 25 µl Pct Recovery = 96% Analysis Date = 08/26/16 SpikeMix = NSI 041816AVOC: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 110% Analysis Date = 08/12/16 SpikeMix = ChemService 5082900: 25 µl & Phenova B20160319: 25 µl Pct Recovery = 106% Analysis Date = 06/30/16 SpikeMix = Crescent 03FF058: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 99% Analysis Date = 03/19/15 SpikeMix = Spex Organics C1140417015: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 104% Analysis Date = 11/14/14 SpikeMix = Crescent 03DD004: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 92% Analysis Date = 06/10/14 SpikeMix = Crescent 03DD004: 20 µl & NSI 032614: 20 µl Pct Recovery = 102% Analysis Date = 07/13/15 SpikeMix = Crescent 04EE008: 25 µl & NSI 050515AVOC: 25 µl Pct Recovery = 80% Analysis Date = 09/29/15 SpikeMix = Accu 215041380: 25 µl & ERA 0406-15-03: 25 µl Pct Recovery = 93% Analysis Date = 06/16/15 SpikeMix = ERA 0406-15-03: 25 µl & Supelco LC13545: 25 µl Pct Recovery = 92% Analysis Date = 11/29/16 SpikeMix = ChemService 5082900: 15 µl & Phenova B20160319: 15 µl Pct Recovery = 110% Analysis Date = 10/13/16 SpikeMix = NSI 041816AVOC: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 100% Analysis Date = 09/28/16 SpikeMix = Crescent 03FF058: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 108% Analysis Date = 06/30/16 SpikeMix = ChemService 5082900: 15 µl & Accu 216041125: 15 µl Pct Recovery = 99% Analysis Date = 06/10/16 SpikeMix = NSI 041816AVOC: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 128% Analysis Date = 05/27/16 SpikeMix = Phenova B20160319: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 89% Analysis Date = 01/13/15 SpikeMix = Accu 214031115: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 106% Analysis Date = 09/09/14 SpikeMix = Accu 214031115: 10 µl & NSI 032614: 10 µl Pct Recovery = 113% Analysis Date = 07/23/14 SpikeMix = Spex Organics C1140417015: 10 µl & Accu 214031115: 10 µl Pct Recovery = 130% Analysis Date = 11/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 81% Analysis Date = 10/17/15 SpikeMix = Crescent 04EE008: 15 µl & NSI 050515AVOC: 15 µl Pct Recovery = 77% Analysis Date = 06/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Accu 215041380: 15 µl Pct Recovery = 85% Analysis Date = 04/26/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 93% Analysis Date = 03/04/16 SpikeMix = Accu 215041380: 15 µl & ERA 0406-15-03: 15 µl Pct Recovery = 99% Analysis Date = 02/05/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 99% Analysis Date = 10/16/15 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 96% Analysis Date = 11/06/14 SpikeMix = Spex Organics C1140417015: 10 µl & Crescent 03DD004: 10 µl Pct Recovery = 96% Analysis Date = 10/04/14 SpikeMix = Crescent 03DD004: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 98% Analysis Date = 07/29/14 SpikeMix = Crescent 03DD004: 10 µl & NSI 032614: 10 µl Pct Recovery = 97% Analysis Date = 03/17/16 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 82% Analysis Date = 01/27/16 SpikeMix = Crescent 04EE008: 10 µl & NSI 050515AVOC: 10 µl Pct Recovery = 83% Analysis Date = 12/10/15 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 89% Analysis Date = 09/03/15 SpikeMix = NSI 050515AVOC: 10 µl & Spex Organics EN150428007: 10 µl Pct Recovery = 76% Analysis Date = 11/20/15 SpikeMix = Accu 215041380: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 106% Analysis Date = 07/31/15 SpikeMix = Crescent 04EE008: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 98% Analysis Date = 06/27/15 SpikeMix = ERA 0406-15-03: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 100% Analysis Date = 12/15/16 Pct Recovery = 106% Analysis Date = 12/11/16 Pct Recovery = 106% Analysis Date = 12/11/16 Pct Recovery = 106% Analysis Date = 12/06/16 Pct Recovery = 106% Analysis Date = 12/06/16 Pct Recovery = 106% Analysis Date = 12/01/16 Pct Recovery = 106% Analysis Date = 12/01/16 Pct Recovery = 106% Analysis Date = 11/26/16 Pct Recovery = 106% Analysis Date = 11/26/16 Pct Recovery = 106% Analysis Date = 11/21/16 Pct Recovery = 105% Analysis Date = 11/21/16 Pct Recovery = 105% Analysis Date = 11/17/16 Pct Recovery = 105% Analysis Date = 11/17/16 Pct Recovery = 105% Analysis Date = 11/12/16 Pct Recovery = 105% Analysis Date = 11/12/16 Pct Recovery = 105% Analysis Date = 11/07/16 Pct Recovery = 105% Analysis Date = 11/07/16 Pct Recovery = 105% Analysis Date = 11/02/16 Pct Recovery = 104% Analysis Date = 11/02/16 Pct Recovery = 104% Analysis Date = 10/28/16 Pct Recovery = 104% Analysis Date = 10/28/16 Pct Recovery = 104% Analysis Date = 10/24/16 Pct Recovery = 104% Analysis Date = 10/24/16 Pct Recovery = 104% Analysis Date = 10/19/16 Pct Recovery = 104% Analysis Date = 10/19/16 Pct Recovery = 104% Analysis Date = 10/14/16 Pct Recovery = 104% Analysis Date = 10/14/16 Pct Recovery = 104% Analysis Date = 10/09/16 Pct Recovery = 103% Analysis Date = 10/09/16 Pct Recovery = 103% Analysis Date = 10/04/16 Pct Recovery = 103% Analysis Date = 10/04/16 Pct Recovery = 103% Analysis Date = 09/30/16 Pct Recovery = 103% Analysis Date = 09/30/16 Pct Recovery = 103% Analysis Date = 09/25/16 Pct Recovery = 103% Analysis Date = 09/25/16 Pct Recovery = 103% Analysis Date = 09/20/16 Pct Recovery = 103% Analysis Date = 09/20/16 Pct Recovery = 103% Analysis Date = 09/15/16 Pct Recovery = 102% Analysis Date = 09/15/16 Pct Recovery = 102% Analysis Date = 09/10/16 Pct Recovery = 102% Analysis Date = 09/10/16 Pct Recovery = 102% Analysis Date = 09/06/16 Pct Recovery = 102% Analysis Date = 09/06/16 Pct Recovery = 102% Analysis Date = 09/01/16 Pct Recovery = 102% Analysis Date = 09/01/16 Pct Recovery = 102% Analysis Date = 08/27/16 Pct Recovery = 102% Analysis Date = 08/27/16 Pct Recovery = 102% Analysis Date = 08/22/16 Pct Recovery = 101% Analysis Date = 08/22/16 Pct Recovery = 101% Analysis Date = 08/17/16 Pct Recovery = 101% Analysis Date = 08/17/16 Pct Recovery = 101% Analysis Date = 08/13/16 Pct Recovery = 101% Analysis Date = 08/13/16 Pct Recovery = 101% Analysis Date = 08/08/16 Pct Recovery = 101% Analysis Date = 08/08/16 Pct Recovery = 101% Analysis Date = 08/03/16 Pct Recovery = 100% Analysis Date = 08/03/16 Pct Recovery = 100% Analysis Date = 07/29/16 Pct Recovery = 100% Analysis Date = 07/29/16 Pct Recovery = 100% Analysis Date = 07/24/16 Pct Recovery = 100% Analysis Date = 07/24/16 Pct Recovery = 100% Analysis Date = 07/20/16 Pct Recovery = 100% Analysis Date = 07/20/16 Pct Recovery = 100% Analysis Date = 07/15/16 Pct Recovery = 100% Analysis Date = 07/15/16 Pct Recovery = 100% Analysis Date = 07/10/16 Pct Recovery = 99% Analysis Date = 07/10/16 Pct Recovery = 99% Analysis Date = 07/05/16 Pct Recovery = 99% Analysis Date = 07/05/16 Pct Recovery = 99% Analysis Date = 06/30/16 Pct Recovery = 99% Analysis Date = 06/30/16 Pct Recovery = 99% Analysis Date = 06/26/16 Pct Recovery = 99% Analysis Date = 06/26/16 Pct Recovery = 99% Analysis Date = 06/21/16 Pct Recovery = 99% Analysis Date = 06/21/16 Pct Recovery = 99% Analysis Date = 06/16/16 Pct Recovery = 98% Analysis Date = 06/16/16 Pct Recovery = 98% Analysis Date = 06/11/16 Pct Recovery = 98% Analysis Date = 06/11/16 Pct Recovery = 98% Analysis Date = 06/06/16 Pct Recovery = 98% Analysis Date = 06/06/16 Pct Recovery = 98% Analysis Date = 06/02/16 Pct Recovery = 98% Analysis Date = 06/02/16 Pct Recovery = 98% Analysis Date = 05/28/16 Pct Recovery = 98% Analysis Date = 05/28/16 Pct Recovery = 98% Analysis Date = 05/23/16 Pct Recovery = 97% Analysis Date = 05/23/16 Pct Recovery = 97% Analysis Date = 05/18/16 Pct Recovery = 97% Analysis Date = 05/18/16 Pct Recovery = 97% Analysis Date = 05/13/16 Pct Recovery = 97% Analysis Date = 05/13/16 Pct Recovery = 97% Analysis Date = 05/09/16 Pct Recovery = 97% Analysis Date = 05/09/16 Pct Recovery = 97% Analysis Date = 05/04/16 Pct Recovery = 97% Analysis Date = 05/04/16 Pct Recovery = 97% Analysis Date = 04/29/16 Pct Recovery = 96% Analysis Date = 04/29/16 Pct Recovery = 96% Analysis Date = 04/24/16 Pct Recovery = 96% Analysis Date = 04/24/16 Pct Recovery = 96% Analysis Date = 04/19/16 Pct Recovery = 96% Analysis Date = 04/19/16 Pct Recovery = 96% Analysis Date = 04/15/16 Pct Recovery = 96% Analysis Date = 04/15/16 Pct Recovery = 96% Analysis Date = 04/10/16 Pct Recovery = 96% Analysis Date = 04/10/16 Pct Recovery = 96% Analysis Date = 04/05/16 Pct Recovery = 95% Analysis Date = 04/05/16 Pct Recovery = 95% Analysis Date = 03/31/16 Pct Recovery = 95% Analysis Date = 03/31/16 Pct Recovery = 95% Analysis Date = 03/26/16 Pct Recovery = 95% Analysis Date = 03/26/16 Pct Recovery = 95% Analysis Date = 03/22/16 Pct Recovery = 95% Analysis Date = 03/22/16 Pct Recovery = 95% Analysis Date = 03/17/16 Pct Recovery = 95% Analysis Date = 03/17/16 Pct Recovery = 95% Analysis Date = 03/12/16 Pct Recovery = 94% Analysis Date = 03/12/16 Pct Recovery = 94% Analysis Date = 03/07/16 Pct Recovery = 94% Analysis Date = 03/07/16 Pct Recovery = 94% Analysis Date = 03/02/16 Pct Recovery = 94% Analysis Date = 03/02/16 Pct Recovery = 94% Analysis Date = 02/27/16 Pct Recovery = 94% Analysis Date = 02/27/16 Pct Recovery = 94% Analysis Date = 02/22/16 Pct Recovery = 94% Analysis Date = 02/22/16 Pct Recovery = 94% Analysis Date = 02/17/16 Pct Recovery = 94% Analysis Date = 02/17/16 Pct Recovery = 94% Analysis Date = 02/12/16 Pct Recovery = 93% Analysis Date = 02/12/16 Pct Recovery = 93% Analysis Date = 02/07/16 Pct Recovery = 93% Analysis Date = 02/07/16 Pct Recovery = 93% Analysis Date = 02/03/16 Pct Recovery = 93% Analysis Date = 02/03/16 Pct Recovery = 93% Analysis Date = 01/29/16 Pct Recovery = 93% Analysis Date = 01/29/16 Pct Recovery = 93% Analysis Date = 01/24/16 Pct Recovery = 93% Analysis Date = 01/24/16 Pct Recovery = 93% Analysis Date = 01/19/16 Pct Recovery = 93% Analysis Date = 01/19/16 Pct Recovery = 93% Analysis Date = 01/14/16 Pct Recovery = 92% Analysis Date = 01/14/16 Pct Recovery = 92% Analysis Date = 01/10/16 Pct Recovery = 92% Analysis Date = 01/10/16 Pct Recovery = 92% Analysis Date = 01/05/16 Pct Recovery = 92% Analysis Date = 01/05/16 Pct Recovery = 92% Analysis Date = 12/31/15 Pct Recovery = 92% Analysis Date = 12/31/15 Pct Recovery = 92% Analysis Date = 12/26/15 Pct Recovery = 92% Analysis Date = 12/26/15 Pct Recovery = 92% Analysis Date = 12/21/15 Pct Recovery = 91% Analysis Date = 12/21/15 Pct Recovery = 91% Analysis Date = 12/17/15 Pct Recovery = 91% Analysis Date = 12/17/15 Pct Recovery = 91% Analysis Date = 12/12/15 Pct Recovery = 91% Analysis Date = 12/12/15 Pct Recovery = 91% Analysis Date = 12/07/15 Pct Recovery = 91% Analysis Date = 12/07/15 Pct Recovery = 91% Analysis Date = 12/02/15 Pct Recovery = 91% Analysis Date = 12/02/15 Pct Recovery = 91% Analysis Date = 11/27/15 Pct Recovery = 91% Analysis Date = 11/27/15 Pct Recovery = 91% Analysis Date = 11/23/15 Pct Recovery = 91% Analysis Date = 11/23/15 Pct Recovery = 91% Analysis Date = 11/18/15 Pct Recovery = 91% Analysis Date = 11/18/15 Pct Recovery = 91% Analysis Date = 11/13/15 Pct Recovery = 91% Analysis Date = 11/13/15 Pct Recovery = 91% Analysis Date = 11/08/15 Pct Recovery = 91% Analysis Date = 11/08/15 Pct Recovery = 91% Analysis Date = 11/03/15 Pct Recovery = 91% Analysis Date = 11/03/15 Pct Recovery = 91% Analysis Date = 10/30/15 Pct Recovery = 91% Analysis Date = 10/30/15 Pct Recovery = 91% Analysis Date = 10/25/15 Pct Recovery = 91% Analysis Date = 10/25/15 Pct Recovery = 91% Analysis Date = 10/20/15 Pct Recovery = 91% Analysis Date = 10/20/15 Pct Recovery = 91% Analysis Date = 10/15/15 Pct Recovery = 91% Analysis Date = 10/15/15 Pct Recovery = 91% Analysis Date = 10/10/15 Pct Recovery = 91% Analysis Date = 10/10/15 Pct Recovery = 91% Analysis Date = 10/06/15 Pct Recovery = 91% Analysis Date = 10/06/15 Pct Recovery = 91% Analysis Date = 10/01/15 Pct Recovery = 91% Analysis Date = 10/01/15 Pct Recovery = 91% Analysis Date = 09/26/15 Pct Recovery = 91% Analysis Date = 09/26/15 Pct Recovery = 91% Analysis Date = 09/21/15 Pct Recovery = 91% Analysis Date = 09/21/15 Pct Recovery = 91% Analysis Date = 09/16/15 Pct Recovery = 91% Analysis Date = 09/16/15 Pct Recovery = 91% Analysis Date = 09/12/15 Pct Recovery = 91% Analysis Date = 09/12/15 Pct Recovery = 91% Analysis Date = 09/07/15 Pct Recovery = 91% Analysis Date = 09/07/15 Pct Recovery = 91% Analysis Date = 09/02/15 Pct Recovery = 91% Analysis Date = 09/02/15 Pct Recovery = 91% Analysis Date = 08/28/15 Pct Recovery = 91% Analysis Date = 08/28/15 Pct Recovery = 91% Analysis Date = 08/23/15 Pct Recovery = 92% Analysis Date = 08/23/15 Pct Recovery = 92% Analysis Date = 08/19/15 Pct Recovery = 92% Analysis Date = 08/19/15 Pct Recovery = 92% Analysis Date = 08/14/15 Pct Recovery = 92% Analysis Date = 08/14/15 Pct Recovery = 92% Analysis Date = 08/09/15 Pct Recovery = 92% Analysis Date = 08/09/15 Pct Recovery = 92% Analysis Date = 08/04/15 Pct Recovery = 92% Analysis Date = 08/04/15 Pct Recovery = 92% Analysis Date = 07/30/15 Pct Recovery = 92% Analysis Date = 07/30/15 Pct Recovery = 92% Analysis Date = 07/26/15 Pct Recovery = 92% Analysis Date = 07/26/15 Pct Recovery = 92% Analysis Date = 07/21/15 Pct Recovery = 92% Analysis Date = 07/21/15 Pct Recovery = 92% Analysis Date = 07/16/15 Pct Recovery = 92% Analysis Date = 07/16/15 Pct Recovery = 92% Analysis Date = 07/11/15 Pct Recovery = 92% Analysis Date = 07/11/15 Pct Recovery = 92% Analysis Date = 07/06/15 Pct Recovery = 93% Analysis Date = 07/06/15 Pct Recovery = 93% Analysis Date = 07/02/15 Pct Recovery = 93% Analysis Date = 07/02/15 Pct Recovery = 93% Analysis Date = 06/27/15 Pct Recovery = 93% Analysis Date = 06/27/15 Pct Recovery = 93% Analysis Date = 06/22/15 Pct Recovery = 93% Analysis Date = 06/22/15 Pct Recovery = 93% Analysis Date = 06/17/15 Pct Recovery = 93% Analysis Date = 06/17/15 Pct Recovery = 93% Analysis Date = 06/12/15 Pct Recovery = 93% Analysis Date = 06/12/15 Pct Recovery = 93% Analysis Date = 06/08/15 Pct Recovery = 93% Analysis Date = 06/08/15 Pct Recovery = 93% Analysis Date = 06/03/15 Pct Recovery = 93% Analysis Date = 06/03/15 Pct Recovery = 93% Analysis Date = 05/29/15 Pct Recovery = 94% Analysis Date = 05/29/15 Pct Recovery = 94% Analysis Date = 05/24/15 Pct Recovery = 94% Analysis Date = 05/24/15 Pct Recovery = 94% Analysis Date = 05/19/15 Pct Recovery = 94% Analysis Date = 05/19/15 Pct Recovery = 94% Analysis Date = 05/15/15 Pct Recovery = 94% Analysis Date = 05/15/15 Pct Recovery = 94% Analysis Date = 05/10/15 Pct Recovery = 94% Analysis Date = 05/10/15 Pct Recovery = 94% Analysis Date = 05/05/15 Pct Recovery = 95% Analysis Date = 05/05/15 Pct Recovery = 95% Analysis Date = 04/30/15 Pct Recovery = 95% Analysis Date = 04/30/15 Pct Recovery = 95% Analysis Date = 04/25/15 Pct Recovery = 95% Analysis Date = 04/25/15 Pct Recovery = 95% Analysis Date = 04/21/15 Pct Recovery = 95% Analysis Date = 04/21/15 Pct Recovery = 95% Analysis Date = 04/16/15 Pct Recovery = 95% Analysis Date = 04/16/15 Pct Recovery = 95% Analysis Date = 04/11/15 Pct Recovery = 95% Analysis Date = 04/11/15 Pct Recovery = 95% Analysis Date = 04/06/15 Pct Recovery = 96% Analysis Date = 04/06/15 Pct Recovery = 96% Analysis Date = 04/01/15 Pct Recovery = 96% Analysis Date = 04/01/15 Pct Recovery = 96% Analysis Date = 03/28/15 Pct Recovery = 96% Analysis Date = 03/28/15 Pct Recovery = 96% Analysis Date = 03/23/15 Pct Recovery = 96% Analysis Date = 03/23/15 Pct Recovery = 96% Analysis Date = 03/18/15 Pct Recovery = 96% Analysis Date = 03/18/15 Pct Recovery = 96% Analysis Date = 03/13/15 Pct Recovery = 97% Analysis Date = 03/13/15 Pct Recovery = 97% Analysis Date = 03/08/15 Pct Recovery = 97% Analysis Date = 03/08/15 Pct Recovery = 97% Analysis Date = 03/04/15 Pct Recovery = 97% Analysis Date = 03/04/15 Pct Recovery = 97% Analysis Date = 02/27/15 Pct Recovery = 97% Analysis Date = 02/27/15 Pct Recovery = 97% Analysis Date = 02/22/15 Pct Recovery = 97% Analysis Date = 02/22/15 Pct Recovery = 97% Analysis Date = 02/17/15 Pct Recovery = 97% Analysis Date = 02/17/15 Pct Recovery = 97% Analysis Date = 02/12/15 Pct Recovery = 98% Analysis Date = 02/12/15 Pct Recovery = 98% Analysis Date = 02/08/15 Pct Recovery = 98% Analysis Date = 02/08/15 Pct Recovery = 98% Analysis Date = 02/03/15 Pct Recovery = 98% Analysis Date = 02/03/15 Pct Recovery = 98% Analysis Date = 01/29/15 Pct Recovery = 98% Analysis Date = 01/29/15 Pct Recovery = 98% Analysis Date = 01/24/15 Pct Recovery = 98% Analysis Date = 01/24/15 Pct Recovery = 98% Analysis Date = 01/19/15 Pct Recovery = 99% Analysis Date = 01/19/15 Pct Recovery = 99% Analysis Date = 01/15/15 Pct Recovery = 99% Analysis Date = 01/15/15 Pct Recovery = 99% Analysis Date = 01/10/15 Pct Recovery = 99% Analysis Date = 01/10/15 Pct Recovery = 99% Analysis Date = 01/05/15 Pct Recovery = 99% Analysis Date = 01/05/15 Pct Recovery = 99% Analysis Date = 12/31/14 Pct Recovery = 99% Analysis Date = 12/31/14 Pct Recovery = 99% Analysis Date = 12/26/14 Pct Recovery = 99% Analysis Date = 12/26/14 Pct Recovery = 99% Analysis Date = 12/22/14 Pct Recovery = 100% Analysis Date = 12/22/14 Pct Recovery = 100% Analysis Date = 12/17/14 Pct Recovery = 100% Analysis Date = 12/17/14 Pct Recovery = 100% Analysis Date = 12/12/14 Pct Recovery = 100% Analysis Date = 12/12/14 Pct Recovery = 100% Analysis Date = 12/07/14 Pct Recovery = 100% Analysis Date = 12/07/14 Pct Recovery = 100% Analysis Date = 12/02/14 Pct Recovery = 100% Analysis Date = 12/02/14 Pct Recovery = 100% Analysis Date = 11/28/14 Pct Recovery = 100% Analysis Date = 11/28/14 Pct Recovery = 100% Analysis Date = 11/23/14 Pct Recovery = 101% Analysis Date = 11/23/14 Pct Recovery = 101% Analysis Date = 11/18/14 Pct Recovery = 101% Analysis Date = 11/18/14 Pct Recovery = 101% Analysis Date = 11/13/14 Pct Recovery = 101% Analysis Date = 11/13/14 Pct Recovery = 101% Analysis Date = 11/08/14 Pct Recovery = 101% Analysis Date = 11/08/14 Pct Recovery = 101% Analysis Date = 11/04/14 Pct Recovery = 101% Analysis Date = 11/04/14 Pct Recovery = 101% Analysis Date = 10/30/14 Pct Recovery = 102% Analysis Date = 10/30/14 Pct Recovery = 102% Analysis Date = 10/25/14 Pct Recovery = 102% Analysis Date = 10/25/14 Pct Recovery = 102% Analysis Date = 10/20/14 Pct Recovery = 102% Analysis Date = 10/20/14 Pct Recovery = 102% Analysis Date = 10/15/14 Pct Recovery = 102% Analysis Date = 10/15/14 Pct Recovery = 102% Analysis Date = 10/11/14 Pct Recovery = 102% Analysis Date = 10/11/14 Pct Recovery = 102% Analysis Date = 10/06/14 Pct Recovery = 102% Analysis Date = 10/06/14 Pct Recovery = 102% Analysis Date = 10/01/14 Pct Recovery = 103% Analysis Date = 10/01/14 Pct Recovery = 103% Analysis Date = 09/26/14 Pct Recovery = 103% Analysis Date = 09/26/14 Pct Recovery = 103% Analysis Date = 09/21/14 Pct Recovery = 103% Analysis Date = 09/21/14 Pct Recovery = 103% Analysis Date = 09/17/14 Pct Recovery = 103% Analysis Date = 09/17/14 Pct Recovery = 103% Analysis Date = 09/12/14 Pct Recovery = 103% Analysis Date = 09/12/14 Pct Recovery = 103% Analysis Date = 09/07/14 Pct Recovery = 103% Analysis Date = 09/07/14 Pct Recovery = 103% Analysis Date = 09/02/14 Pct Recovery = 104% Analysis Date = 09/02/14 Pct Recovery = 104% Analysis Date = 08/28/14 Pct Recovery = 104% Analysis Date = 08/28/14 Pct Recovery = 104% Analysis Date = 08/24/14 Pct Recovery = 104% Analysis Date = 08/24/14 Pct Recovery = 104% Analysis Date = 08/19/14 Pct Recovery = 104% Analysis Date = 08/19/14 Pct Recovery = 104% Analysis Date = 08/14/14 Pct Recovery = 104% Analysis Date = 08/14/14 Pct Recovery = 104% Analysis Date = 08/09/14 Pct Recovery = 105% Analysis Date = 08/09/14 Pct Recovery = 105% Analysis Date = 08/04/14 Pct Recovery = 105% Analysis Date = 08/04/14 Pct Recovery = 105% Analysis Date = 07/31/14 Pct Recovery = 105% Analysis Date = 07/31/14 Pct Recovery = 105% Analysis Date = 07/26/14 Pct Recovery = 105% Analysis Date = 07/26/14 Pct Recovery = 105% Analysis Date = 07/21/14 Pct Recovery = 105% Analysis Date = 07/21/14 Pct Recovery = 105% Analysis Date = 07/16/14 Pct Recovery = 105% Analysis Date = 07/16/14 Pct Recovery = 105% Analysis Date = 07/11/14 Pct Recovery = 106% Analysis Date = 07/11/14 Pct Recovery = 106% Analysis Date = 07/07/14 Pct Recovery = 106% Analysis Date = 07/07/14 Pct Recovery = 106% Analysis Date = 07/02/14 Pct Recovery = 106% Analysis Date = 07/02/14 Pct Recovery = 106% Analysis Date = 06/27/14 Pct Recovery = 106% Analysis Date = 06/27/14 Pct Recovery = 106% Analysis Date = 06/22/14 Pct Recovery = 106% Analysis Date = 06/22/14 Pct Recovery = 106% Analysis Date = 06/17/14 Pct Recovery = 106% Analysis Date = 06/17/14 Pct Recovery = 106% Analysis Date = 06/13/14 Pct Recovery = 107% Analysis Date = 06/13/14 Pct Recovery = 107% Analysis Date = 06/08/14 Pct Recovery = 107% Analysis Date = 06/08/14 Pct Recovery = 107% Analysis Date = 06/03/14 Pct Recovery = 107% Analysis Date = 06/03/14 Pct Recovery = 107% Analysis Date = 05/29/14 Pct Recovery = 107% Analysis Date = 05/29/14 Pct Recovery = 107% Analysis Date = 05/24/14 Pct Recovery = 107% Analysis Date = 05/24/14 Pct Recovery = 107% Analysis Date = 05/20/14 Pct Recovery = 107% Analysis Date = 05/20/14 Pct Recovery = 107% Analysis Date = 05/15/14 Pct Recovery = 108% Analysis Date = 05/15/14 Pct Recovery = 108% Analysis Date = 05/10/14 Pct Recovery = 108% Analysis Date = 05/10/14 Pct Recovery = 108% Analysis Date = 05/05/14 Pct Recovery = 108% Analysis Date = 05/05/14 Pct Recovery = 108% Analysis Date = 05/01/14 Pct Recovery = 108% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
BENZENE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 44 98% 12% 98% 9%
Total 44 98% 12% 98% 9%

Sample Statistics
BENZENE

Characteristic N % % Basis
Plotted 44 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 44 .  
False Negatives 0 0% 0 out of 44
Not Spiked 21 .  
False Positives 1 5% 1 out of 21

BQS OBSP Determination:
BROMOBENZENE
METHOD: 4440 , TESTIDCODE: 81555GCM66
Open Data Set

Analysis Date = 12/16/16 SpikeMix = NSI 041816AVOC: 40 µl & ChemService 5082900: 40 µl Pct Recovery = 127% Analysis Date = 12/12/16 SpikeMix = Accu 216041125: 40 µl & Crescent 03FF058: 40 µl Pct Recovery = 103% Analysis Date = 08/04/16 SpikeMix = Crescent 03FF058: 40 µl & Supelco LC20141V: 40 µl Pct Recovery = 89% Analysis Date = 07/14/16 SpikeMix = Accu 216041125: 40 µl & NSI 041816AVOC: 40 µl Pct Recovery = 131% Analysis Date = 11/21/16 SpikeMix = Crescent 03FF058: 25 µl & Supelco LC20141V: 25 µl Pct Recovery = 98% Analysis Date = 08/26/16 SpikeMix = NSI 041816AVOC: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 119% Analysis Date = 06/30/16 SpikeMix = Crescent 03FF058: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 96% Analysis Date = 06/21/16 SpikeMix = Phenova B20160319: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 105% Analysis Date = 05/24/16 SpikeMix = Accu 216041125: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 100% Analysis Date = 03/19/15 SpikeMix = Spex Organics C1140417015: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 102% Analysis Date = 03/06/15 SpikeMix = ERA 0227-14-06.1A: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 95% Analysis Date = 12/17/14 SpikeMix = Supelco LC06438: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 103% Analysis Date = 11/22/14 SpikeMix = NSI 032614: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 98% Analysis Date = 09/21/14 SpikeMix = Supelco LC06438: 20 µl Pct Recovery = 98% Analysis Date = 08/19/14 SpikeMix = Spex Organics C1140417015: 20 µl & Accu 214031115: 20 µl Pct Recovery = 97% Analysis Date = 08/16/14 SpikeMix = ERA 0227-14-06.1A: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 88% Analysis Date = 06/10/14 SpikeMix = NSI 032614: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 92% Analysis Date = 09/29/15 SpikeMix = Accu 215041380: 25 µl & ERA 0406-15-03: 25 µl Pct Recovery = 92% Analysis Date = 08/15/15 SpikeMix = Supelco LC13545: 25 µl & Crescent 04EE008: 25 µl Pct Recovery = 98% Analysis Date = 07/13/15 SpikeMix = Crescent 04EE008: 25 µl & NSI 050515AVOC: 25 µl Pct Recovery = 94% Analysis Date = 10/13/16 SpikeMix = Accu 216041125: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 131% Analysis Date = 10/13/16 SpikeMix = NSI 041816AVOC: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 124% Analysis Date = 09/28/16 SpikeMix = Crescent 03FF058: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 96% Analysis Date = 09/08/16 SpikeMix = Phenova B20160319: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 97% Analysis Date = 08/20/16 SpikeMix = Accu 216041125: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 92% Analysis Date = 07/29/16 SpikeMix = Phenova B20160319: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 117% Analysis Date = 06/10/16 SpikeMix = NSI 041816AVOC: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 121% Analysis Date = 04/02/16 SpikeMix = Supelco LC13545: 15 µl & Accu 215041380: 15 µl Pct Recovery = 96% Analysis Date = 03/04/16 SpikeMix = Accu 215041380: 15 µl & ERA 0406-15-03: 15 µl Pct Recovery = 91% Analysis Date = 06/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Accu 215041380: 15 µl Pct Recovery = 91% Analysis Date = 12/18/15 SpikeMix = Supelco LC13545: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 105% Analysis Date = 10/17/15 SpikeMix = Crescent 04EE008: 15 µl & NSI 050515AVOC: 15 µl Pct Recovery = 89% Analysis Date = 05/09/15 SpikeMix = Spex Organics EN150428007: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 96% Analysis Date = 11/06/14 SpikeMix = Spex Organics C1140417015: 10 µl & Crescent 03DD004: 10 µl Pct Recovery = 105% Analysis Date = 10/21/14 SpikeMix = ERA 0227-14-06.1A: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 100% Analysis Date = 09/09/14 SpikeMix = NSI 032614: 10 µl & Spex Organics C1140417015: 10 µl Pct Recovery = 105% Analysis Date = 07/23/14 SpikeMix = Spex Organics C1140417015: 10 µl & Accu 214031115: 10 µl Pct Recovery = 94% Analysis Date = 07/11/14 SpikeMix = Spex Organics C1140417015: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 90% Analysis Date = 06/18/14 SpikeMix = Supelco LC06438: 10 µl & Accu 214031115: 10 µl Pct Recovery = 98% Analysis Date = 05/30/14 SpikeMix = NSI 032614: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 93% Analysis Date = 05/03/14 SpikeMix = Crescent 03DD004: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 103% Analysis Date = 02/18/16 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 101% Analysis Date = 11/20/15 SpikeMix = Accu 215041380: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 106% Analysis Date = 11/12/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 89% Analysis Date = 05/21/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 120% Analysis Date = 05/13/16 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 111% Analysis Date = 01/27/16 SpikeMix = Crescent 04EE008: 10 µl & NSI 050515AVOC: 10 µl Pct Recovery = 99% Analysis Date = 07/31/15 SpikeMix = Crescent 04EE008: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 89% Analysis Date = 05/09/15 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 96% Analysis Date = 12/16/16 Pct Recovery = 113% Analysis Date = 12/11/16 Pct Recovery = 113% Analysis Date = 12/11/16 Pct Recovery = 113% Analysis Date = 12/06/16 Pct Recovery = 113% Analysis Date = 12/06/16 Pct Recovery = 113% Analysis Date = 12/01/16 Pct Recovery = 113% Analysis Date = 12/01/16 Pct Recovery = 113% Analysis Date = 11/26/16 Pct Recovery = 113% Analysis Date = 11/26/16 Pct Recovery = 113% Analysis Date = 11/22/16 Pct Recovery = 112% Analysis Date = 11/22/16 Pct Recovery = 112% Analysis Date = 11/17/16 Pct Recovery = 112% Analysis Date = 11/17/16 Pct Recovery = 112% Analysis Date = 11/12/16 Pct Recovery = 112% Analysis Date = 11/12/16 Pct Recovery = 112% Analysis Date = 11/07/16 Pct Recovery = 112% Analysis Date = 11/07/16 Pct Recovery = 112% Analysis Date = 11/02/16 Pct Recovery = 112% Analysis Date = 11/02/16 Pct Recovery = 112% Analysis Date = 10/29/16 Pct Recovery = 111% Analysis Date = 10/29/16 Pct Recovery = 111% Analysis Date = 10/24/16 Pct Recovery = 111% Analysis Date = 10/24/16 Pct Recovery = 111% Analysis Date = 10/19/16 Pct Recovery = 111% Analysis Date = 10/19/16 Pct Recovery = 111% Analysis Date = 10/14/16 Pct Recovery = 111% Analysis Date = 10/14/16 Pct Recovery = 111% Analysis Date = 10/09/16 Pct Recovery = 111% Analysis Date = 10/09/16 Pct Recovery = 111% Analysis Date = 10/05/16 Pct Recovery = 110% Analysis Date = 10/05/16 Pct Recovery = 110% Analysis Date = 09/30/16 Pct Recovery = 110% Analysis Date = 09/30/16 Pct Recovery = 110% Analysis Date = 09/25/16 Pct Recovery = 110% Analysis Date = 09/25/16 Pct Recovery = 110% Analysis Date = 09/20/16 Pct Recovery = 110% Analysis Date = 09/20/16 Pct Recovery = 110% Analysis Date = 09/15/16 Pct Recovery = 110% Analysis Date = 09/15/16 Pct Recovery = 110% Analysis Date = 09/11/16 Pct Recovery = 109% Analysis Date = 09/11/16 Pct Recovery = 109% Analysis Date = 09/06/16 Pct Recovery = 109% Analysis Date = 09/06/16 Pct Recovery = 109% Analysis Date = 09/01/16 Pct Recovery = 109% Analysis Date = 09/01/16 Pct Recovery = 109% Analysis Date = 08/27/16 Pct Recovery = 109% Analysis Date = 08/27/16 Pct Recovery = 109% Analysis Date = 08/23/16 Pct Recovery = 109% Analysis Date = 08/23/16 Pct Recovery = 109% Analysis Date = 08/18/16 Pct Recovery = 108% Analysis Date = 08/18/16 Pct Recovery = 108% Analysis Date = 08/13/16 Pct Recovery = 108% Analysis Date = 08/13/16 Pct Recovery = 108% Analysis Date = 08/08/16 Pct Recovery = 108% Analysis Date = 08/08/16 Pct Recovery = 108% Analysis Date = 08/03/16 Pct Recovery = 108% Analysis Date = 08/03/16 Pct Recovery = 108% Analysis Date = 07/30/16 Pct Recovery = 108% Analysis Date = 07/30/16 Pct Recovery = 108% Analysis Date = 07/25/16 Pct Recovery = 107% Analysis Date = 07/25/16 Pct Recovery = 107% Analysis Date = 07/20/16 Pct Recovery = 107% Analysis Date = 07/20/16 Pct Recovery = 107% Analysis Date = 07/15/16 Pct Recovery = 107% Analysis Date = 07/15/16 Pct Recovery = 107% Analysis Date = 07/10/16 Pct Recovery = 107% Analysis Date = 07/10/16 Pct Recovery = 107% Analysis Date = 07/06/16 Pct Recovery = 106% Analysis Date = 07/06/16 Pct Recovery = 106% Analysis Date = 07/01/16 Pct Recovery = 106% Analysis Date = 07/01/16 Pct Recovery = 106% Analysis Date = 06/26/16 Pct Recovery = 106% Analysis Date = 06/26/16 Pct Recovery = 106% Analysis Date = 06/21/16 Pct Recovery = 106% Analysis Date = 06/21/16 Pct Recovery = 106% Analysis Date = 06/16/16 Pct Recovery = 106% Analysis Date = 06/16/16 Pct Recovery = 106% Analysis Date = 06/12/16 Pct Recovery = 105% Analysis Date = 06/12/16 Pct Recovery = 105% Analysis Date = 06/07/16 Pct Recovery = 105% Analysis Date = 06/07/16 Pct Recovery = 105% Analysis Date = 06/02/16 Pct Recovery = 105% Analysis Date = 06/02/16 Pct Recovery = 105% Analysis Date = 05/28/16 Pct Recovery = 105% Analysis Date = 05/28/16 Pct Recovery = 105% Analysis Date = 05/24/16 Pct Recovery = 105% Analysis Date = 05/24/16 Pct Recovery = 105% Analysis Date = 05/19/16 Pct Recovery = 104% Analysis Date = 05/19/16 Pct Recovery = 104% Analysis Date = 05/14/16 Pct Recovery = 104% Analysis Date = 05/14/16 Pct Recovery = 104% Analysis Date = 05/09/16 Pct Recovery = 104% Analysis Date = 05/09/16 Pct Recovery = 104% Analysis Date = 05/04/16 Pct Recovery = 104% Analysis Date = 05/04/16 Pct Recovery = 104% Analysis Date = 04/30/16 Pct Recovery = 104% Analysis Date = 04/30/16 Pct Recovery = 104% Analysis Date = 04/25/16 Pct Recovery = 103% Analysis Date = 04/25/16 Pct Recovery = 103% Analysis Date = 04/20/16 Pct Recovery = 103% Analysis Date = 04/20/16 Pct Recovery = 103% Analysis Date = 04/15/16 Pct Recovery = 103% Analysis Date = 04/15/16 Pct Recovery = 103% Analysis Date = 04/10/16 Pct Recovery = 103% Analysis Date = 04/10/16 Pct Recovery = 103% Analysis Date = 04/06/16 Pct Recovery = 103% Analysis Date = 04/06/16 Pct Recovery = 103% Analysis Date = 04/01/16 Pct Recovery = 102% Analysis Date = 04/01/16 Pct Recovery = 102% Analysis Date = 03/27/16 Pct Recovery = 102% Analysis Date = 03/27/16 Pct Recovery = 102% Analysis Date = 03/22/16 Pct Recovery = 102% Analysis Date = 03/22/16 Pct Recovery = 102% Analysis Date = 03/17/16 Pct Recovery = 102% Analysis Date = 03/17/16 Pct Recovery = 102% Analysis Date = 03/13/16 Pct Recovery = 102% Analysis Date = 03/13/16 Pct Recovery = 102% Analysis Date = 03/08/16 Pct Recovery = 101% Analysis Date = 03/08/16 Pct Recovery = 101% Analysis Date = 03/03/16 Pct Recovery = 101% Analysis Date = 03/03/16 Pct Recovery = 101% Analysis Date = 02/27/16 Pct Recovery = 101% Analysis Date = 02/27/16 Pct Recovery = 101% Analysis Date = 02/23/16 Pct Recovery = 101% Analysis Date = 02/23/16 Pct Recovery = 101% Analysis Date = 02/18/16 Pct Recovery = 101% Analysis Date = 02/18/16 Pct Recovery = 101% Analysis Date = 02/13/16 Pct Recovery = 100% Analysis Date = 02/13/16 Pct Recovery = 100% Analysis Date = 02/08/16 Pct Recovery = 100% Analysis Date = 02/08/16 Pct Recovery = 100% Analysis Date = 02/03/16 Pct Recovery = 100% Analysis Date = 02/03/16 Pct Recovery = 100% Analysis Date = 01/30/16 Pct Recovery = 100% Analysis Date = 01/30/16 Pct Recovery = 100% Analysis Date = 01/25/16 Pct Recovery = 100% Analysis Date = 01/25/16 Pct Recovery = 100% Analysis Date = 01/20/16 Pct Recovery = 100% Analysis Date = 01/20/16 Pct Recovery = 100% Analysis Date = 01/15/16 Pct Recovery = 100% Analysis Date = 01/15/16 Pct Recovery = 100% Analysis Date = 01/10/16 Pct Recovery = 99% Analysis Date = 01/10/16 Pct Recovery = 99% Analysis Date = 01/06/16 Pct Recovery = 99% Analysis Date = 01/06/16 Pct Recovery = 99% Analysis Date = 01/01/16 Pct Recovery = 99% Analysis Date = 01/01/16 Pct Recovery = 99% Analysis Date = 12/27/15 Pct Recovery = 99% Analysis Date = 12/27/15 Pct Recovery = 99% Analysis Date = 12/22/15 Pct Recovery = 99% Analysis Date = 12/22/15 Pct Recovery = 99% Analysis Date = 12/17/15 Pct Recovery = 99% Analysis Date = 12/17/15 Pct Recovery = 99% Analysis Date = 12/13/15 Pct Recovery = 98% Analysis Date = 12/13/15 Pct Recovery = 98% Analysis Date = 12/08/15 Pct Recovery = 98% Analysis Date = 12/08/15 Pct Recovery = 98% Analysis Date = 12/03/15 Pct Recovery = 98% Analysis Date = 12/03/15 Pct Recovery = 98% Analysis Date = 11/28/15 Pct Recovery = 98% Analysis Date = 11/28/15 Pct Recovery = 98% Analysis Date = 11/24/15 Pct Recovery = 98% Analysis Date = 11/24/15 Pct Recovery = 98% Analysis Date = 11/19/15 Pct Recovery = 98% Analysis Date = 11/19/15 Pct Recovery = 98% Analysis Date = 11/14/15 Pct Recovery = 98% Analysis Date = 11/14/15 Pct Recovery = 98% Analysis Date = 11/09/15 Pct Recovery = 98% Analysis Date = 11/09/15 Pct Recovery = 98% Analysis Date = 11/04/15 Pct Recovery = 98% Analysis Date = 11/04/15 Pct Recovery = 98% Analysis Date = 10/31/15 Pct Recovery = 98% Analysis Date = 10/31/15 Pct Recovery = 98% Analysis Date = 10/26/15 Pct Recovery = 98% Analysis Date = 10/26/15 Pct Recovery = 98% Analysis Date = 10/21/15 Pct Recovery = 98% Analysis Date = 10/21/15 Pct Recovery = 98% Analysis Date = 10/16/15 Pct Recovery = 98% Analysis Date = 10/16/15 Pct Recovery = 98% Analysis Date = 10/11/15 Pct Recovery = 98% Analysis Date = 10/11/15 Pct Recovery = 98% Analysis Date = 10/07/15 Pct Recovery = 98% Analysis Date = 10/07/15 Pct Recovery = 98% Analysis Date = 10/02/15 Pct Recovery = 98% Analysis Date = 10/02/15 Pct Recovery = 98% Analysis Date = 09/27/15 Pct Recovery = 98% Analysis Date = 09/27/15 Pct Recovery = 98% Analysis Date = 09/22/15 Pct Recovery = 98% Analysis Date = 09/22/15 Pct Recovery = 98% Analysis Date = 09/17/15 Pct Recovery = 98% Analysis Date = 09/17/15 Pct Recovery = 98% Analysis Date = 09/13/15 Pct Recovery = 98% Analysis Date = 09/13/15 Pct Recovery = 98% Analysis Date = 09/08/15 Pct Recovery = 98% Analysis Date = 09/08/15 Pct Recovery = 98% Analysis Date = 09/03/15 Pct Recovery = 98% Analysis Date = 09/03/15 Pct Recovery = 98% Analysis Date = 08/29/15 Pct Recovery = 98% Analysis Date = 08/29/15 Pct Recovery = 98% Analysis Date = 08/25/15 Pct Recovery = 98% Analysis Date = 08/25/15 Pct Recovery = 98% Analysis Date = 08/20/15 Pct Recovery = 98% Analysis Date = 08/20/15 Pct Recovery = 98% Analysis Date = 08/15/15 Pct Recovery = 98% Analysis Date = 08/15/15 Pct Recovery = 98% Analysis Date = 08/10/15 Pct Recovery = 98% Analysis Date = 08/10/15 Pct Recovery = 98% Analysis Date = 08/05/15 Pct Recovery = 97% Analysis Date = 08/05/15 Pct Recovery = 97% Analysis Date = 08/01/15 Pct Recovery = 97% Analysis Date = 08/01/15 Pct Recovery = 97% Analysis Date = 07/27/15 Pct Recovery = 98% Analysis Date = 07/27/15 Pct Recovery = 98% Analysis Date = 07/22/15 Pct Recovery = 98% Analysis Date = 07/22/15 Pct Recovery = 98% Analysis Date = 07/17/15 Pct Recovery = 98% Analysis Date = 07/17/15 Pct Recovery = 98% Analysis Date = 07/12/15 Pct Recovery = 98% Analysis Date = 07/12/15 Pct Recovery = 98% Analysis Date = 07/08/15 Pct Recovery = 98% Analysis Date = 07/08/15 Pct Recovery = 98% Analysis Date = 07/03/15 Pct Recovery = 98% Analysis Date = 07/03/15 Pct Recovery = 98% Analysis Date = 06/28/15 Pct Recovery = 98% Analysis Date = 06/28/15 Pct Recovery = 98% Analysis Date = 06/23/15 Pct Recovery = 98% Analysis Date = 06/23/15 Pct Recovery = 98% Analysis Date = 06/18/15 Pct Recovery = 98% Analysis Date = 06/18/15 Pct Recovery = 98% Analysis Date = 06/14/15 Pct Recovery = 98% Analysis Date = 06/14/15 Pct Recovery = 98% Analysis Date = 06/09/15 Pct Recovery = 98% Analysis Date = 06/09/15 Pct Recovery = 98% Analysis Date = 06/04/15 Pct Recovery = 98% Analysis Date = 06/04/15 Pct Recovery = 98% Analysis Date = 05/30/15 Pct Recovery = 98% Analysis Date = 05/30/15 Pct Recovery = 98% Analysis Date = 05/25/15 Pct Recovery = 98% Analysis Date = 05/25/15 Pct Recovery = 98% Analysis Date = 05/21/15 Pct Recovery = 98% Analysis Date = 05/21/15 Pct Recovery = 98% Analysis Date = 05/16/15 Pct Recovery = 98% Analysis Date = 05/16/15 Pct Recovery = 98% Analysis Date = 05/11/15 Pct Recovery = 98% Analysis Date = 05/11/15 Pct Recovery = 98% Analysis Date = 05/06/15 Pct Recovery = 98% Analysis Date = 05/06/15 Pct Recovery = 98% Analysis Date = 05/02/15 Pct Recovery = 98% Analysis Date = 05/02/15 Pct Recovery = 98% Analysis Date = 04/27/15 Pct Recovery = 98% Analysis Date = 04/27/15 Pct Recovery = 98% Analysis Date = 04/22/15 Pct Recovery = 98% Analysis Date = 04/22/15 Pct Recovery = 98% Analysis Date = 04/17/15 Pct Recovery = 98% Analysis Date = 04/17/15 Pct Recovery = 98% Analysis Date = 04/12/15 Pct Recovery = 98% Analysis Date = 04/12/15 Pct Recovery = 98% Analysis Date = 04/08/15 Pct Recovery = 98% Analysis Date = 04/08/15 Pct Recovery = 98% Analysis Date = 04/03/15 Pct Recovery = 98% Analysis Date = 04/03/15 Pct Recovery = 98% Analysis Date = 03/29/15 Pct Recovery = 98% Analysis Date = 03/29/15 Pct Recovery = 98% Analysis Date = 03/24/15 Pct Recovery = 98% Analysis Date = 03/24/15 Pct Recovery = 98% Analysis Date = 03/19/15 Pct Recovery = 98% Analysis Date = 03/19/15 Pct Recovery = 98% Analysis Date = 03/15/15 Pct Recovery = 98% Analysis Date = 03/15/15 Pct Recovery = 98% Analysis Date = 03/10/15 Pct Recovery = 98% Analysis Date = 03/10/15 Pct Recovery = 98% Analysis Date = 03/05/15 Pct Recovery = 98% Analysis Date = 03/05/15 Pct Recovery = 98% Analysis Date = 02/28/15 Pct Recovery = 98% Analysis Date = 02/28/15 Pct Recovery = 98% Analysis Date = 02/23/15 Pct Recovery = 98% Analysis Date = 02/23/15 Pct Recovery = 98% Analysis Date = 02/19/15 Pct Recovery = 98% Analysis Date = 02/19/15 Pct Recovery = 98% Analysis Date = 02/14/15 Pct Recovery = 98% Analysis Date = 02/14/15 Pct Recovery = 98% Analysis Date = 02/09/15 Pct Recovery = 98% Analysis Date = 02/09/15 Pct Recovery = 98% Analysis Date = 02/04/15 Pct Recovery = 98% Analysis Date = 02/04/15 Pct Recovery = 98% Analysis Date = 01/31/15 Pct Recovery = 98% Analysis Date = 01/31/15 Pct Recovery = 98% Analysis Date = 01/26/15 Pct Recovery = 98% Analysis Date = 01/26/15 Pct Recovery = 98% Analysis Date = 01/21/15 Pct Recovery = 98% Analysis Date = 01/21/15 Pct Recovery = 98% Analysis Date = 01/16/15 Pct Recovery = 98% Analysis Date = 01/16/15 Pct Recovery = 98% Analysis Date = 01/11/15 Pct Recovery = 98% Analysis Date = 01/11/15 Pct Recovery = 98% Analysis Date = 01/07/15 Pct Recovery = 98% Analysis Date = 01/07/15 Pct Recovery = 98% Analysis Date = 01/02/15 Pct Recovery = 98% Analysis Date = 01/02/15 Pct Recovery = 98% Analysis Date = 12/28/14 Pct Recovery = 98% Analysis Date = 12/28/14 Pct Recovery = 98% Analysis Date = 12/23/14 Pct Recovery = 98% Analysis Date = 12/23/14 Pct Recovery = 98% Analysis Date = 12/18/14 Pct Recovery = 98% Analysis Date = 12/18/14 Pct Recovery = 98% Analysis Date = 12/14/14 Pct Recovery = 98% Analysis Date = 12/14/14 Pct Recovery = 98% Analysis Date = 12/09/14 Pct Recovery = 98% Analysis Date = 12/09/14 Pct Recovery = 98% Analysis Date = 12/04/14 Pct Recovery = 98% Analysis Date = 12/04/14 Pct Recovery = 98% Analysis Date = 11/29/14 Pct Recovery = 98% Analysis Date = 11/29/14 Pct Recovery = 98% Analysis Date = 11/24/14 Pct Recovery = 98% Analysis Date = 11/24/14 Pct Recovery = 98% Analysis Date = 11/20/14 Pct Recovery = 98% Analysis Date = 11/20/14 Pct Recovery = 98% Analysis Date = 11/15/14 Pct Recovery = 98% Analysis Date = 11/15/14 Pct Recovery = 98% Analysis Date = 11/10/14 Pct Recovery = 98% Analysis Date = 11/10/14 Pct Recovery = 98% Analysis Date = 11/05/14 Pct Recovery = 98% Analysis Date = 11/05/14 Pct Recovery = 98% Analysis Date = 11/01/14 Pct Recovery = 97% Analysis Date = 11/01/14 Pct Recovery = 97% Analysis Date = 10/27/14 Pct Recovery = 97% Analysis Date = 10/27/14 Pct Recovery = 97% Analysis Date = 10/22/14 Pct Recovery = 97% Analysis Date = 10/22/14 Pct Recovery = 97% Analysis Date = 10/17/14 Pct Recovery = 97% Analysis Date = 10/17/14 Pct Recovery = 97% Analysis Date = 10/12/14 Pct Recovery = 97% Analysis Date = 10/12/14 Pct Recovery = 97% Analysis Date = 10/08/14 Pct Recovery = 97% Analysis Date = 10/08/14 Pct Recovery = 97% Analysis Date = 10/03/14 Pct Recovery = 97% Analysis Date = 10/03/14 Pct Recovery = 97% Analysis Date = 09/28/14 Pct Recovery = 97% Analysis Date = 09/28/14 Pct Recovery = 97% Analysis Date = 09/23/14 Pct Recovery = 97% Analysis Date = 09/23/14 Pct Recovery = 97% Analysis Date = 09/18/14 Pct Recovery = 97% Analysis Date = 09/18/14 Pct Recovery = 97% Analysis Date = 09/14/14 Pct Recovery = 97% Analysis Date = 09/14/14 Pct Recovery = 97% Analysis Date = 09/09/14 Pct Recovery = 97% Analysis Date = 09/09/14 Pct Recovery = 97% Analysis Date = 09/04/14 Pct Recovery = 97% Analysis Date = 09/04/14 Pct Recovery = 97% Analysis Date = 08/30/14 Pct Recovery = 97% Analysis Date = 08/30/14 Pct Recovery = 97% Analysis Date = 08/25/14 Pct Recovery = 97% Analysis Date = 08/25/14 Pct Recovery = 97% Analysis Date = 08/21/14 Pct Recovery = 97% Analysis Date = 08/21/14 Pct Recovery = 97% Analysis Date = 08/16/14 Pct Recovery = 97% Analysis Date = 08/16/14 Pct Recovery = 97% Analysis Date = 08/11/14 Pct Recovery = 97% Analysis Date = 08/11/14 Pct Recovery = 97% Analysis Date = 08/06/14 Pct Recovery = 97% Analysis Date = 08/06/14 Pct Recovery = 97% Analysis Date = 08/02/14 Pct Recovery = 97% Analysis Date = 08/02/14 Pct Recovery = 97% Analysis Date = 07/28/14 Pct Recovery = 97% Analysis Date = 07/28/14 Pct Recovery = 97% Analysis Date = 07/23/14 Pct Recovery = 97% Analysis Date = 07/23/14 Pct Recovery = 97% Analysis Date = 07/18/14 Pct Recovery = 97% Analysis Date = 07/18/14 Pct Recovery = 97% Analysis Date = 07/13/14 Pct Recovery = 97% Analysis Date = 07/13/14 Pct Recovery = 97% Analysis Date = 07/09/14 Pct Recovery = 97% Analysis Date = 07/09/14 Pct Recovery = 97% Analysis Date = 07/04/14 Pct Recovery = 97% Analysis Date = 07/04/14 Pct Recovery = 97% Analysis Date = 06/29/14 Pct Recovery = 97% Analysis Date = 06/29/14 Pct Recovery = 97% Analysis Date = 06/24/14 Pct Recovery = 97% Analysis Date = 06/24/14 Pct Recovery = 97% Analysis Date = 06/19/14 Pct Recovery = 97% Analysis Date = 06/19/14 Pct Recovery = 97% Analysis Date = 06/15/14 Pct Recovery = 97% Analysis Date = 06/15/14 Pct Recovery = 97% Analysis Date = 06/10/14 Pct Recovery = 97% Analysis Date = 06/10/14 Pct Recovery = 97% Analysis Date = 06/05/14 Pct Recovery = 96% Analysis Date = 06/05/14 Pct Recovery = 96% Analysis Date = 05/31/14 Pct Recovery = 96% Analysis Date = 05/31/14 Pct Recovery = 96% Analysis Date = 05/26/14 Pct Recovery = 96% Analysis Date = 05/26/14 Pct Recovery = 96% Analysis Date = 05/22/14 Pct Recovery = 96% Analysis Date = 05/22/14 Pct Recovery = 96% Analysis Date = 05/17/14 Pct Recovery = 96% Analysis Date = 05/17/14 Pct Recovery = 96% Analysis Date = 05/12/14 Pct Recovery = 96% Analysis Date = 05/12/14 Pct Recovery = 96% Analysis Date = 05/07/14 Pct Recovery = 96% Analysis Date = 05/07/14 Pct Recovery = 96% Analysis Date = 05/03/14 Pct Recovery = 96% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
BROMOBENZENE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 49 101% 11% 98% 8%
Total 49 101% 11% 98% 8%

Sample Statistics
BROMOBENZENE

Characteristic N % % Basis
Plotted 49 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 49 .  
False Negatives 0 0% 0 out of 49
Not Spiked 24 .  
False Positives 0 0% 0 out of 24

BQS OBSP Determination:
BROMOCHLOROMETHANE
METHOD: 4440 , TESTIDCODE: 77297GCM66
Open Data Set

Analysis Date = 12/16/16 SpikeMix = NSI 041816AVOC: 40 µl & ChemService 5082900: 40 µl Pct Recovery = 117% Analysis Date = 08/04/16 SpikeMix = Crescent 03FF058: 40 µl & Supelco LC20141V: 40 µl Pct Recovery = 124% Analysis Date = 07/20/16 SpikeMix = Supelco LC20141V: 40 µl & Accu 216041125: 40 µl Pct Recovery = 92% Analysis Date = 08/26/16 SpikeMix = NSI 041816AVOC: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 122% Analysis Date = 08/12/16 SpikeMix = ChemService 5082900: 25 µl & Phenova B20160319: 25 µl Pct Recovery = 113% Analysis Date = 06/30/16 SpikeMix = Crescent 03FF058: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 138% Analysis Date = 11/21/16 SpikeMix = Crescent 03FF058: 25 µl & Supelco LC20141V: 25 µl Pct Recovery = 116% Analysis Date = 09/08/16 SpikeMix = Supelco LC20141V: 25 µl & Accu 216041125: 25 µl Pct Recovery = 112% Analysis Date = 03/06/15 SpikeMix = ERA 0227-14-06.1A: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 99% Analysis Date = 12/17/14 SpikeMix = Supelco LC06438: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 99% Analysis Date = 09/21/14 SpikeMix = Supelco LC06438: 20 µl Pct Recovery = 87% Analysis Date = 06/10/14 SpikeMix = NSI 032614: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 94% Analysis Date = 03/19/15 SpikeMix = Spex Organics C1140417015: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 108% Analysis Date = 11/22/14 SpikeMix = NSI 032614: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 98% Analysis Date = 08/19/14 SpikeMix = Spex Organics C1140417015: 20 µl & Accu 214031115: 20 µl Pct Recovery = 101% Analysis Date = 08/16/14 SpikeMix = ERA 0227-14-06.1A: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 112% Analysis Date = 08/15/15 SpikeMix = Supelco LC13545: 25 µl & Crescent 04EE008: 25 µl Pct Recovery = 103% Analysis Date = 07/13/15 SpikeMix = Crescent 04EE008: 25 µl & NSI 050515AVOC: 25 µl Pct Recovery = 99% Analysis Date = 09/29/15 SpikeMix = Accu 215041380: 25 µl & ERA 0406-15-03: 25 µl Pct Recovery = 95% Analysis Date = 11/29/16 SpikeMix = ChemService 5082900: 15 µl & Phenova B20160319: 15 µl Pct Recovery = 104% Analysis Date = 09/28/16 SpikeMix = Crescent 03FF058: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 132% Analysis Date = 06/30/16 SpikeMix = ChemService 5082900: 15 µl & Accu 216041125: 15 µl Pct Recovery = 115% Analysis Date = 06/10/16 SpikeMix = NSI 041816AVOC: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 111% Analysis Date = 10/13/16 SpikeMix = NSI 041816AVOC: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 104% Analysis Date = 05/27/16 SpikeMix = Phenova B20160319: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 100% Analysis Date = 12/18/15 SpikeMix = Supelco LC13545: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 94% Analysis Date = 10/17/15 SpikeMix = Crescent 04EE008: 15 µl & NSI 050515AVOC: 15 µl Pct Recovery = 107% Analysis Date = 05/09/15 SpikeMix = Spex Organics EN150428007: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 103% Analysis Date = 04/02/16 SpikeMix = Supelco LC13545: 15 µl & Accu 215041380: 15 µl Pct Recovery = 103% Analysis Date = 03/04/16 SpikeMix = Accu 215041380: 15 µl & ERA 0406-15-03: 15 µl Pct Recovery = 88% Analysis Date = 06/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Accu 215041380: 15 µl Pct Recovery = 86% Analysis Date = 10/21/14 SpikeMix = ERA 0227-14-06.1A: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 99% Analysis Date = 06/18/14 SpikeMix = Supelco LC06438: 10 µl & Accu 214031115: 10 µl Pct Recovery = 100% Analysis Date = 05/30/14 SpikeMix = NSI 032614: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 84% Analysis Date = 05/03/14 SpikeMix = Crescent 03DD004: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 105% Analysis Date = 11/06/14 SpikeMix = Spex Organics C1140417015: 10 µl & Crescent 03DD004: 10 µl Pct Recovery = 95% Analysis Date = 09/09/14 SpikeMix = NSI 032614: 10 µl & Spex Organics C1140417015: 10 µl Pct Recovery = 102% Analysis Date = 07/23/14 SpikeMix = Spex Organics C1140417015: 10 µl & Accu 214031115: 10 µl Pct Recovery = 106% Analysis Date = 07/11/14 SpikeMix = Spex Organics C1140417015: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 101% Analysis Date = 05/13/16 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 103% Analysis Date = 01/27/16 SpikeMix = Crescent 04EE008: 10 µl & NSI 050515AVOC: 10 µl Pct Recovery = 111% Analysis Date = 07/31/15 SpikeMix = Crescent 04EE008: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 86% Analysis Date = 05/09/15 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 96% Analysis Date = 02/18/16 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 89% Analysis Date = 11/20/15 SpikeMix = Accu 215041380: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 103% Analysis Date = 11/12/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 99% Analysis Date = 05/21/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 105% Analysis Date = 12/16/16 Pct Recovery = 118% Analysis Date = 12/11/16 Pct Recovery = 118% Analysis Date = 12/11/16 Pct Recovery = 118% Analysis Date = 12/06/16 Pct Recovery = 118% Analysis Date = 12/06/16 Pct Recovery = 118% Analysis Date = 12/01/16 Pct Recovery = 118% Analysis Date = 12/01/16 Pct Recovery = 118% Analysis Date = 11/26/16 Pct Recovery = 117% Analysis Date = 11/26/16 Pct Recovery = 117% Analysis Date = 11/22/16 Pct Recovery = 117% Analysis Date = 11/22/16 Pct Recovery = 117% Analysis Date = 11/17/16 Pct Recovery = 117% Analysis Date = 11/17/16 Pct Recovery = 117% Analysis Date = 11/12/16 Pct Recovery = 117% Analysis Date = 11/12/16 Pct Recovery = 117% Analysis Date = 11/07/16 Pct Recovery = 116% Analysis Date = 11/07/16 Pct Recovery = 116% Analysis Date = 11/02/16 Pct Recovery = 116% Analysis Date = 11/02/16 Pct Recovery = 116% Analysis Date = 10/29/16 Pct Recovery = 116% Analysis Date = 10/29/16 Pct Recovery = 116% Analysis Date = 10/24/16 Pct Recovery = 116% Analysis Date = 10/24/16 Pct Recovery = 116% Analysis Date = 10/19/16 Pct Recovery = 115% Analysis Date = 10/19/16 Pct Recovery = 115% Analysis Date = 10/14/16 Pct Recovery = 115% Analysis Date = 10/14/16 Pct Recovery = 115% Analysis Date = 10/09/16 Pct Recovery = 115% Analysis Date = 10/09/16 Pct Recovery = 115% Analysis Date = 10/05/16 Pct Recovery = 115% Analysis Date = 10/05/16 Pct Recovery = 115% Analysis Date = 09/30/16 Pct Recovery = 114% Analysis Date = 09/30/16 Pct Recovery = 114% Analysis Date = 09/25/16 Pct Recovery = 114% Analysis Date = 09/25/16 Pct Recovery = 114% Analysis Date = 09/20/16 Pct Recovery = 114% Analysis Date = 09/20/16 Pct Recovery = 114% Analysis Date = 09/15/16 Pct Recovery = 114% Analysis Date = 09/15/16 Pct Recovery = 114% Analysis Date = 09/11/16 Pct Recovery = 114% Analysis Date = 09/11/16 Pct Recovery = 114% Analysis Date = 09/06/16 Pct Recovery = 113% Analysis Date = 09/06/16 Pct Recovery = 113% Analysis Date = 09/01/16 Pct Recovery = 113% Analysis Date = 09/01/16 Pct Recovery = 113% Analysis Date = 08/27/16 Pct Recovery = 113% Analysis Date = 08/27/16 Pct Recovery = 113% Analysis Date = 08/23/16 Pct Recovery = 113% Analysis Date = 08/23/16 Pct Recovery = 113% Analysis Date = 08/18/16 Pct Recovery = 112% Analysis Date = 08/18/16 Pct Recovery = 112% Analysis Date = 08/13/16 Pct Recovery = 112% Analysis Date = 08/13/16 Pct Recovery = 112% Analysis Date = 08/08/16 Pct Recovery = 112% Analysis Date = 08/08/16 Pct Recovery = 112% Analysis Date = 08/03/16 Pct Recovery = 112% Analysis Date = 08/03/16 Pct Recovery = 112% Analysis Date = 07/30/16 Pct Recovery = 111% Analysis Date = 07/30/16 Pct Recovery = 111% Analysis Date = 07/25/16 Pct Recovery = 111% Analysis Date = 07/25/16 Pct Recovery = 111% Analysis Date = 07/20/16 Pct Recovery = 111% Analysis Date = 07/20/16 Pct Recovery = 111% Analysis Date = 07/15/16 Pct Recovery = 111% Analysis Date = 07/15/16 Pct Recovery = 111% Analysis Date = 07/10/16 Pct Recovery = 110% Analysis Date = 07/10/16 Pct Recovery = 110% Analysis Date = 07/06/16 Pct Recovery = 110% Analysis Date = 07/06/16 Pct Recovery = 110% Analysis Date = 07/01/16 Pct Recovery = 110% Analysis Date = 07/01/16 Pct Recovery = 110% Analysis Date = 06/26/16 Pct Recovery = 110% Analysis Date = 06/26/16 Pct Recovery = 110% Analysis Date = 06/21/16 Pct Recovery = 109% Analysis Date = 06/21/16 Pct Recovery = 109% Analysis Date = 06/16/16 Pct Recovery = 109% Analysis Date = 06/16/16 Pct Recovery = 109% Analysis Date = 06/12/16 Pct Recovery = 109% Analysis Date = 06/12/16 Pct Recovery = 109% Analysis Date = 06/07/16 Pct Recovery = 109% Analysis Date = 06/07/16 Pct Recovery = 109% Analysis Date = 06/02/16 Pct Recovery = 109% Analysis Date = 06/02/16 Pct Recovery = 109% Analysis Date = 05/28/16 Pct Recovery = 108% Analysis Date = 05/28/16 Pct Recovery = 108% Analysis Date = 05/24/16 Pct Recovery = 108% Analysis Date = 05/24/16 Pct Recovery = 108% Analysis Date = 05/19/16 Pct Recovery = 108% Analysis Date = 05/19/16 Pct Recovery = 108% Analysis Date = 05/14/16 Pct Recovery = 108% Analysis Date = 05/14/16 Pct Recovery = 108% Analysis Date = 05/09/16 Pct Recovery = 107% Analysis Date = 05/09/16 Pct Recovery = 107% Analysis Date = 05/04/16 Pct Recovery = 107% Analysis Date = 05/04/16 Pct Recovery = 107% Analysis Date = 04/30/16 Pct Recovery = 107% Analysis Date = 04/30/16 Pct Recovery = 107% Analysis Date = 04/25/16 Pct Recovery = 107% Analysis Date = 04/25/16 Pct Recovery = 107% Analysis Date = 04/20/16 Pct Recovery = 106% Analysis Date = 04/20/16 Pct Recovery = 106% Analysis Date = 04/15/16 Pct Recovery = 106% Analysis Date = 04/15/16 Pct Recovery = 106% Analysis Date = 04/10/16 Pct Recovery = 106% Analysis Date = 04/10/16 Pct Recovery = 106% Analysis Date = 04/06/16 Pct Recovery = 106% Analysis Date = 04/06/16 Pct Recovery = 106% Analysis Date = 04/01/16 Pct Recovery = 105% Analysis Date = 04/01/16 Pct Recovery = 105% Analysis Date = 03/27/16 Pct Recovery = 105% Analysis Date = 03/27/16 Pct Recovery = 105% Analysis Date = 03/22/16 Pct Recovery = 105% Analysis Date = 03/22/16 Pct Recovery = 105% Analysis Date = 03/17/16 Pct Recovery = 105% Analysis Date = 03/17/16 Pct Recovery = 105% Analysis Date = 03/13/16 Pct Recovery = 104% Analysis Date = 03/13/16 Pct Recovery = 104% Analysis Date = 03/08/16 Pct Recovery = 104% Analysis Date = 03/08/16 Pct Recovery = 104% Analysis Date = 03/03/16 Pct Recovery = 104% Analysis Date = 03/03/16 Pct Recovery = 104% Analysis Date = 02/27/16 Pct Recovery = 104% Analysis Date = 02/27/16 Pct Recovery = 104% Analysis Date = 02/23/16 Pct Recovery = 103% Analysis Date = 02/23/16 Pct Recovery = 103% Analysis Date = 02/18/16 Pct Recovery = 103% Analysis Date = 02/18/16 Pct Recovery = 103% Analysis Date = 02/13/16 Pct Recovery = 103% Analysis Date = 02/13/16 Pct Recovery = 103% Analysis Date = 02/08/16 Pct Recovery = 103% Analysis Date = 02/08/16 Pct Recovery = 103% Analysis Date = 02/03/16 Pct Recovery = 102% Analysis Date = 02/03/16 Pct Recovery = 102% Analysis Date = 01/30/16 Pct Recovery = 102% Analysis Date = 01/30/16 Pct Recovery = 102% Analysis Date = 01/25/16 Pct Recovery = 102% Analysis Date = 01/25/16 Pct Recovery = 102% Analysis Date = 01/20/16 Pct Recovery = 102% Analysis Date = 01/20/16 Pct Recovery = 102% Analysis Date = 01/15/16 Pct Recovery = 102% Analysis Date = 01/15/16 Pct Recovery = 102% Analysis Date = 01/10/16 Pct Recovery = 101% Analysis Date = 01/10/16 Pct Recovery = 101% Analysis Date = 01/06/16 Pct Recovery = 101% Analysis Date = 01/06/16 Pct Recovery = 101% Analysis Date = 01/01/16 Pct Recovery = 101% Analysis Date = 01/01/16 Pct Recovery = 101% Analysis Date = 12/27/15 Pct Recovery = 101% Analysis Date = 12/27/15 Pct Recovery = 101% Analysis Date = 12/22/15 Pct Recovery = 101% Analysis Date = 12/22/15 Pct Recovery = 101% Analysis Date = 12/17/15 Pct Recovery = 100% Analysis Date = 12/17/15 Pct Recovery = 100% Analysis Date = 12/13/15 Pct Recovery = 100% Analysis Date = 12/13/15 Pct Recovery = 100% Analysis Date = 12/08/15 Pct Recovery = 100% Analysis Date = 12/08/15 Pct Recovery = 100% Analysis Date = 12/03/15 Pct Recovery = 100% Analysis Date = 12/03/15 Pct Recovery = 100% Analysis Date = 11/28/15 Pct Recovery = 100% Analysis Date = 11/28/15 Pct Recovery = 100% Analysis Date = 11/24/15 Pct Recovery = 99% Analysis Date = 11/24/15 Pct Recovery = 99% Analysis Date = 11/19/15 Pct Recovery = 99% Analysis Date = 11/19/15 Pct Recovery = 99% Analysis Date = 11/14/15 Pct Recovery = 99% Analysis Date = 11/14/15 Pct Recovery = 99% Analysis Date = 11/09/15 Pct Recovery = 99% Analysis Date = 11/09/15 Pct Recovery = 99% Analysis Date = 11/04/15 Pct Recovery = 99% Analysis Date = 11/04/15 Pct Recovery = 99% Analysis Date = 10/31/15 Pct Recovery = 99% Analysis Date = 10/31/15 Pct Recovery = 99% Analysis Date = 10/26/15 Pct Recovery = 99% Analysis Date = 10/26/15 Pct Recovery = 99% Analysis Date = 10/21/15 Pct Recovery = 99% Analysis Date = 10/21/15 Pct Recovery = 99% Analysis Date = 10/16/15 Pct Recovery = 99% Analysis Date = 10/16/15 Pct Recovery = 99% Analysis Date = 10/11/15 Pct Recovery = 99% Analysis Date = 10/11/15 Pct Recovery = 99% Analysis Date = 10/07/15 Pct Recovery = 99% Analysis Date = 10/07/15 Pct Recovery = 99% Analysis Date = 10/02/15 Pct Recovery = 99% Analysis Date = 10/02/15 Pct Recovery = 99% Analysis Date = 09/27/15 Pct Recovery = 99% Analysis Date = 09/27/15 Pct Recovery = 99% Analysis Date = 09/22/15 Pct Recovery = 99% Analysis Date = 09/22/15 Pct Recovery = 99% Analysis Date = 09/17/15 Pct Recovery = 99% Analysis Date = 09/17/15 Pct Recovery = 99% Analysis Date = 09/13/15 Pct Recovery = 99% Analysis Date = 09/13/15 Pct Recovery = 99% Analysis Date = 09/08/15 Pct Recovery = 99% Analysis Date = 09/08/15 Pct Recovery = 99% Analysis Date = 09/03/15 Pct Recovery = 99% Analysis Date = 09/03/15 Pct Recovery = 99% Analysis Date = 08/29/15 Pct Recovery = 99% Analysis Date = 08/29/15 Pct Recovery = 99% Analysis Date = 08/25/15 Pct Recovery = 99% Analysis Date = 08/25/15 Pct Recovery = 99% Analysis Date = 08/20/15 Pct Recovery = 99% Analysis Date = 08/20/15 Pct Recovery = 99% Analysis Date = 08/15/15 Pct Recovery = 99% Analysis Date = 08/15/15 Pct Recovery = 99% Analysis Date = 08/10/15 Pct Recovery = 99% Analysis Date = 08/10/15 Pct Recovery = 99% Analysis Date = 08/05/15 Pct Recovery = 99% Analysis Date = 08/05/15 Pct Recovery = 99% Analysis Date = 08/01/15 Pct Recovery = 99% Analysis Date = 08/01/15 Pct Recovery = 99% Analysis Date = 07/27/15 Pct Recovery = 99% Analysis Date = 07/27/15 Pct Recovery = 99% Analysis Date = 07/22/15 Pct Recovery = 99% Analysis Date = 07/22/15 Pct Recovery = 99% Analysis Date = 07/17/15 Pct Recovery = 99% Analysis Date = 07/17/15 Pct Recovery = 99% Analysis Date = 07/12/15 Pct Recovery = 99% Analysis Date = 07/12/15 Pct Recovery = 99% Analysis Date = 07/08/15 Pct Recovery = 99% Analysis Date = 07/08/15 Pct Recovery = 99% Analysis Date = 07/03/15 Pct Recovery = 99% Analysis Date = 07/03/15 Pct Recovery = 99% Analysis Date = 06/28/15 Pct Recovery = 99% Analysis Date = 06/28/15 Pct Recovery = 99% Analysis Date = 06/23/15 Pct Recovery = 99% Analysis Date = 06/23/15 Pct Recovery = 99% Analysis Date = 06/18/15 Pct Recovery = 99% Analysis Date = 06/18/15 Pct Recovery = 99% Analysis Date = 06/14/15 Pct Recovery = 99% Analysis Date = 06/14/15 Pct Recovery = 99% Analysis Date = 06/09/15 Pct Recovery = 99% Analysis Date = 06/09/15 Pct Recovery = 99% Analysis Date = 06/04/15 Pct Recovery = 98% Analysis Date = 06/04/15 Pct Recovery = 98% Analysis Date = 05/30/15 Pct Recovery = 98% Analysis Date = 05/30/15 Pct Recovery = 98% Analysis Date = 05/25/15 Pct Recovery = 98% Analysis Date = 05/25/15 Pct Recovery = 98% Analysis Date = 05/21/15 Pct Recovery = 98% Analysis Date = 05/21/15 Pct Recovery = 98% Analysis Date = 05/16/15 Pct Recovery = 98% Analysis Date = 05/16/15 Pct Recovery = 98% Analysis Date = 05/11/15 Pct Recovery = 98% Analysis Date = 05/11/15 Pct Recovery = 98% Analysis Date = 05/06/15 Pct Recovery = 98% Analysis Date = 05/06/15 Pct Recovery = 98% Analysis Date = 05/02/15 Pct Recovery = 98% Analysis Date = 05/02/15 Pct Recovery = 98% Analysis Date = 04/27/15 Pct Recovery = 98% Analysis Date = 04/27/15 Pct Recovery = 98% Analysis Date = 04/22/15 Pct Recovery = 98% Analysis Date = 04/22/15 Pct Recovery = 98% Analysis Date = 04/17/15 Pct Recovery = 98% Analysis Date = 04/17/15 Pct Recovery = 98% Analysis Date = 04/12/15 Pct Recovery = 98% Analysis Date = 04/12/15 Pct Recovery = 98% Analysis Date = 04/08/15 Pct Recovery = 98% Analysis Date = 04/08/15 Pct Recovery = 98% Analysis Date = 04/03/15 Pct Recovery = 98% Analysis Date = 04/03/15 Pct Recovery = 98% Analysis Date = 03/29/15 Pct Recovery = 98% Analysis Date = 03/29/15 Pct Recovery = 98% Analysis Date = 03/24/15 Pct Recovery = 98% Analysis Date = 03/24/15 Pct Recovery = 98% Analysis Date = 03/19/15 Pct Recovery = 98% Analysis Date = 03/19/15 Pct Recovery = 98% Analysis Date = 03/15/15 Pct Recovery = 98% Analysis Date = 03/15/15 Pct Recovery = 98% Analysis Date = 03/10/15 Pct Recovery = 98% Analysis Date = 03/10/15 Pct Recovery = 98% Analysis Date = 03/05/15 Pct Recovery = 99% Analysis Date = 03/05/15 Pct Recovery = 99% Analysis Date = 02/28/15 Pct Recovery = 99% Analysis Date = 02/28/15 Pct Recovery = 99% Analysis Date = 02/23/15 Pct Recovery = 99% Analysis Date = 02/23/15 Pct Recovery = 99% Analysis Date = 02/19/15 Pct Recovery = 99% Analysis Date = 02/19/15 Pct Recovery = 99% Analysis Date = 02/14/15 Pct Recovery = 99% Analysis Date = 02/14/15 Pct Recovery = 99% Analysis Date = 02/09/15 Pct Recovery = 99% Analysis Date = 02/09/15 Pct Recovery = 99% Analysis Date = 02/04/15 Pct Recovery = 99% Analysis Date = 02/04/15 Pct Recovery = 99% Analysis Date = 01/31/15 Pct Recovery = 99% Analysis Date = 01/31/15 Pct Recovery = 99% Analysis Date = 01/26/15 Pct Recovery = 99% Analysis Date = 01/26/15 Pct Recovery = 99% Analysis Date = 01/21/15 Pct Recovery = 99% Analysis Date = 01/21/15 Pct Recovery = 99% Analysis Date = 01/16/15 Pct Recovery = 99% Analysis Date = 01/16/15 Pct Recovery = 99% Analysis Date = 01/11/15 Pct Recovery = 99% Analysis Date = 01/11/15 Pct Recovery = 99% Analysis Date = 01/07/15 Pct Recovery = 99% Analysis Date = 01/07/15 Pct Recovery = 99% Analysis Date = 01/02/15 Pct Recovery = 99% Analysis Date = 01/02/15 Pct Recovery = 99% Analysis Date = 12/28/14 Pct Recovery = 99% Analysis Date = 12/28/14 Pct Recovery = 99% Analysis Date = 12/23/14 Pct Recovery = 99% Analysis Date = 12/23/14 Pct Recovery = 99% Analysis Date = 12/18/14 Pct Recovery = 99% Analysis Date = 12/18/14 Pct Recovery = 99% Analysis Date = 12/14/14 Pct Recovery = 99% Analysis Date = 12/14/14 Pct Recovery = 99% Analysis Date = 12/09/14 Pct Recovery = 99% Analysis Date = 12/09/14 Pct Recovery = 99% Analysis Date = 12/04/14 Pct Recovery = 99% Analysis Date = 12/04/14 Pct Recovery = 99% Analysis Date = 11/29/14 Pct Recovery = 99% Analysis Date = 11/29/14 Pct Recovery = 99% Analysis Date = 11/24/14 Pct Recovery = 99% Analysis Date = 11/24/14 Pct Recovery = 99% Analysis Date = 11/20/14 Pct Recovery = 99% Analysis Date = 11/20/14 Pct Recovery = 99% Analysis Date = 11/15/14 Pct Recovery = 99% Analysis Date = 11/15/14 Pct Recovery = 99% Analysis Date = 11/10/14 Pct Recovery = 99% Analysis Date = 11/10/14 Pct Recovery = 99% Analysis Date = 11/05/14 Pct Recovery = 99% Analysis Date = 11/05/14 Pct Recovery = 99% Analysis Date = 11/01/14 Pct Recovery = 99% Analysis Date = 11/01/14 Pct Recovery = 99% Analysis Date = 10/27/14 Pct Recovery = 99% Analysis Date = 10/27/14 Pct Recovery = 99% Analysis Date = 10/22/14 Pct Recovery = 99% Analysis Date = 10/22/14 Pct Recovery = 99% Analysis Date = 10/17/14 Pct Recovery = 99% Analysis Date = 10/17/14 Pct Recovery = 99% Analysis Date = 10/12/14 Pct Recovery = 99% Analysis Date = 10/12/14 Pct Recovery = 99% Analysis Date = 10/08/14 Pct Recovery = 99% Analysis Date = 10/08/14 Pct Recovery = 99% Analysis Date = 10/03/14 Pct Recovery = 99% Analysis Date = 10/03/14 Pct Recovery = 99% Analysis Date = 09/28/14 Pct Recovery = 99% Analysis Date = 09/28/14 Pct Recovery = 99% Analysis Date = 09/23/14 Pct Recovery = 99% Analysis Date = 09/23/14 Pct Recovery = 99% Analysis Date = 09/18/14 Pct Recovery = 99% Analysis Date = 09/18/14 Pct Recovery = 99% Analysis Date = 09/14/14 Pct Recovery = 99% Analysis Date = 09/14/14 Pct Recovery = 99% Analysis Date = 09/09/14 Pct Recovery = 99% Analysis Date = 09/09/14 Pct Recovery = 99% Analysis Date = 09/04/14 Pct Recovery = 99% Analysis Date = 09/04/14 Pct Recovery = 99% Analysis Date = 08/30/14 Pct Recovery = 99% Analysis Date = 08/30/14 Pct Recovery = 99% Analysis Date = 08/25/14 Pct Recovery = 99% Analysis Date = 08/25/14 Pct Recovery = 99% Analysis Date = 08/21/14 Pct Recovery = 99% Analysis Date = 08/21/14 Pct Recovery = 99% Analysis Date = 08/16/14 Pct Recovery = 99% Analysis Date = 08/16/14 Pct Recovery = 99% Analysis Date = 08/11/14 Pct Recovery = 99% Analysis Date = 08/11/14 Pct Recovery = 99% Analysis Date = 08/06/14 Pct Recovery = 99% Analysis Date = 08/06/14 Pct Recovery = 99% Analysis Date = 08/02/14 Pct Recovery = 99% Analysis Date = 08/02/14 Pct Recovery = 99% Analysis Date = 07/28/14 Pct Recovery = 99% Analysis Date = 07/28/14 Pct Recovery = 99% Analysis Date = 07/23/14 Pct Recovery = 99% Analysis Date = 07/23/14 Pct Recovery = 99% Analysis Date = 07/18/14 Pct Recovery = 99% Analysis Date = 07/18/14 Pct Recovery = 99% Analysis Date = 07/13/14 Pct Recovery = 99% Analysis Date = 07/13/14 Pct Recovery = 99% Analysis Date = 07/09/14 Pct Recovery = 99% Analysis Date = 07/09/14 Pct Recovery = 99% Analysis Date = 07/04/14 Pct Recovery = 99% Analysis Date = 07/04/14 Pct Recovery = 99% Analysis Date = 06/29/14 Pct Recovery = 99% Analysis Date = 06/29/14 Pct Recovery = 99% Analysis Date = 06/24/14 Pct Recovery = 99% Analysis Date = 06/24/14 Pct Recovery = 99% Analysis Date = 06/19/14 Pct Recovery = 99% Analysis Date = 06/19/14 Pct Recovery = 99% Analysis Date = 06/15/14 Pct Recovery = 99% Analysis Date = 06/15/14 Pct Recovery = 99% Analysis Date = 06/10/14 Pct Recovery = 99% Analysis Date = 06/10/14 Pct Recovery = 99% Analysis Date = 06/05/14 Pct Recovery = 99% Analysis Date = 06/05/14 Pct Recovery = 99% Analysis Date = 05/31/14 Pct Recovery = 99% Analysis Date = 05/31/14 Pct Recovery = 99% Analysis Date = 05/26/14 Pct Recovery = 99% Analysis Date = 05/26/14 Pct Recovery = 99% Analysis Date = 05/22/14 Pct Recovery = 99% Analysis Date = 05/22/14 Pct Recovery = 99% Analysis Date = 05/17/14 Pct Recovery = 99% Analysis Date = 05/17/14 Pct Recovery = 99% Analysis Date = 05/12/14 Pct Recovery = 99% Analysis Date = 05/12/14 Pct Recovery = 99% Analysis Date = 05/07/14 Pct Recovery = 99% Analysis Date = 05/07/14 Pct Recovery = 99% Analysis Date = 05/03/14 Pct Recovery = 99% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
BROMOCHLOROMETHANE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 47 103% 11% 103% 12%
Total 47 103% 11% 103% 12%

Sample Statistics
BROMOCHLOROMETHANE

Characteristic N % % Basis
Plotted 47 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 47 .  
False Negatives 0 0% 0 out of 47
Not Spiked 26 .  
False Positives 6 23% 6 out of 26

BQS OBSP Determination:
BROMODICHLOROMETHANE
METHOD: 4440 , TESTIDCODE: 32101GCM66
Open Data Set

Analysis Date = 12/16/16 SpikeMix = NSI 041816AVOC: 40 µl & ChemService 5082900: 40 µl Pct Recovery = 125% Analysis Date = 08/04/16 SpikeMix = Crescent 03FF058: 40 µl & Supelco LC20141V: 40 µl Pct Recovery = 90% Analysis Date = 07/20/16 SpikeMix = Supelco LC20141V: 40 µl & Accu 216041125: 40 µl Pct Recovery = 100% Analysis Date = 08/26/16 SpikeMix = NSI 041816AVOC: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 123% Analysis Date = 08/12/16 SpikeMix = ChemService 5082900: 25 µl & Phenova B20160319: 25 µl Pct Recovery = 103% Analysis Date = 06/30/16 SpikeMix = Crescent 03FF058: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 107% Analysis Date = 11/21/16 SpikeMix = Crescent 03FF058: 25 µl & Supelco LC20141V: 25 µl Pct Recovery = 102% Analysis Date = 09/08/16 SpikeMix = Supelco LC20141V: 25 µl & Accu 216041125: 25 µl Pct Recovery = 94% Analysis Date = 11/22/14 SpikeMix = NSI 032614: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 101% Analysis Date = 06/10/14 SpikeMix = Crescent 03DD004: 20 µl & NSI 032614: 20 µl Pct Recovery = 107% Analysis Date = 06/10/14 SpikeMix = NSI 032614: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 111% Analysis Date = 05/01/14 SpikeMix = Accu 214031115: 20 µl & NSI 032614: 20 µl Pct Recovery = 112% Analysis Date = 04/09/15 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 102% Analysis Date = 03/06/15 SpikeMix = ERA 0227-14-06.1A: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 94% Analysis Date = 11/14/14 SpikeMix = Crescent 03DD004: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 89% Analysis Date = 08/16/14 SpikeMix = ERA 0227-14-06.1A: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 98% Analysis Date = 07/01/14 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 101% Analysis Date = 08/15/15 SpikeMix = Supelco LC13545: 25 µl & Crescent 04EE008: 25 µl Pct Recovery = 101% Analysis Date = 06/16/15 SpikeMix = ERA 0406-15-03: 25 µl & Supelco LC13545: 25 µl Pct Recovery = 89% Analysis Date = 11/29/16 SpikeMix = ChemService 5082900: 15 µl & Phenova B20160319: 15 µl Pct Recovery = 109% Analysis Date = 09/28/16 SpikeMix = Crescent 03FF058: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 103% Analysis Date = 06/30/16 SpikeMix = ChemService 5082900: 15 µl & Accu 216041125: 15 µl Pct Recovery = 111% Analysis Date = 06/10/16 SpikeMix = NSI 041816AVOC: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 109% Analysis Date = 10/13/16 SpikeMix = NSI 041816AVOC: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 99% Analysis Date = 05/27/16 SpikeMix = Phenova B20160319: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 102% Analysis Date = 04/26/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 121% Analysis Date = 04/02/16 SpikeMix = Supelco LC13545: 15 µl & Accu 215041380: 15 µl Pct Recovery = 104% Analysis Date = 02/05/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 100% Analysis Date = 12/18/15 SpikeMix = Supelco LC13545: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 90% Analysis Date = 11/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 113% Analysis Date = 10/16/15 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 118% Analysis Date = 05/09/15 SpikeMix = Spex Organics EN150428007: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 112% Analysis Date = 09/09/14 SpikeMix = Accu 214031115: 10 µl & NSI 032614: 10 µl Pct Recovery = 114% Analysis Date = 09/09/14 SpikeMix = NSI 032614: 10 µl & Spex Organics C1140417015: 10 µl Pct Recovery = 102% Analysis Date = 07/29/14 SpikeMix = Crescent 03DD004: 10 µl & NSI 032614: 10 µl Pct Recovery = 121% Analysis Date = 05/30/14 SpikeMix = NSI 032614: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 127% Analysis Date = 01/13/15 SpikeMix = Accu 214031115: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 88% Analysis Date = 10/21/14 SpikeMix = ERA 0227-14-06.1A: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 90% Analysis Date = 10/04/14 SpikeMix = Crescent 03DD004: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 94% Analysis Date = 07/11/14 SpikeMix = Spex Organics C1140417015: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 104% Analysis Date = 05/13/16 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 109% Analysis Date = 03/17/16 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 103% Analysis Date = 02/18/16 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 124% Analysis Date = 12/10/15 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 105% Analysis Date = 11/12/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 113% Analysis Date = 09/03/15 SpikeMix = NSI 050515AVOC: 10 µl & Spex Organics EN150428007: 10 µl Pct Recovery = 107% Analysis Date = 06/27/15 SpikeMix = ERA 0406-15-03: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 100% Analysis Date = 05/21/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 111% Analysis Date = 05/09/15 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 100% Analysis Date = 12/15/16 Pct Recovery = 106% Analysis Date = 12/11/16 Pct Recovery = 106% Analysis Date = 12/11/16 Pct Recovery = 106% Analysis Date = 12/06/16 Pct Recovery = 106% Analysis Date = 12/06/16 Pct Recovery = 106% Analysis Date = 12/01/16 Pct Recovery = 106% Analysis Date = 12/01/16 Pct Recovery = 106% Analysis Date = 11/26/16 Pct Recovery = 106% Analysis Date = 11/26/16 Pct Recovery = 106% Analysis Date = 11/21/16 Pct Recovery = 106% Analysis Date = 11/21/16 Pct Recovery = 106% Analysis Date = 11/17/16 Pct Recovery = 106% Analysis Date = 11/17/16 Pct Recovery = 106% Analysis Date = 11/12/16 Pct Recovery = 106% Analysis Date = 11/12/16 Pct Recovery = 106% Analysis Date = 11/07/16 Pct Recovery = 106% Analysis Date = 11/07/16 Pct Recovery = 106% Analysis Date = 11/02/16 Pct Recovery = 106% Analysis Date = 11/02/16 Pct Recovery = 106% Analysis Date = 10/28/16 Pct Recovery = 106% Analysis Date = 10/28/16 Pct Recovery = 106% Analysis Date = 10/24/16 Pct Recovery = 106% Analysis Date = 10/24/16 Pct Recovery = 106% Analysis Date = 10/19/16 Pct Recovery = 106% Analysis Date = 10/19/16 Pct Recovery = 106% Analysis Date = 10/14/16 Pct Recovery = 106% Analysis Date = 10/14/16 Pct Recovery = 106% Analysis Date = 10/09/16 Pct Recovery = 106% Analysis Date = 10/09/16 Pct Recovery = 106% Analysis Date = 10/04/16 Pct Recovery = 106% Analysis Date = 10/04/16 Pct Recovery = 106% Analysis Date = 09/30/16 Pct Recovery = 106% Analysis Date = 09/30/16 Pct Recovery = 106% Analysis Date = 09/25/16 Pct Recovery = 106% Analysis Date = 09/25/16 Pct Recovery = 106% Analysis Date = 09/20/16 Pct Recovery = 106% Analysis Date = 09/20/16 Pct Recovery = 106% Analysis Date = 09/15/16 Pct Recovery = 106% Analysis Date = 09/15/16 Pct Recovery = 106% Analysis Date = 09/10/16 Pct Recovery = 106% Analysis Date = 09/10/16 Pct Recovery = 106% Analysis Date = 09/06/16 Pct Recovery = 106% Analysis Date = 09/06/16 Pct Recovery = 106% Analysis Date = 09/01/16 Pct Recovery = 106% Analysis Date = 09/01/16 Pct Recovery = 106% Analysis Date = 08/27/16 Pct Recovery = 106% Analysis Date = 08/27/16 Pct Recovery = 106% Analysis Date = 08/22/16 Pct Recovery = 106% Analysis Date = 08/22/16 Pct Recovery = 106% Analysis Date = 08/17/16 Pct Recovery = 106% Analysis Date = 08/17/16 Pct Recovery = 106% Analysis Date = 08/13/16 Pct Recovery = 106% Analysis Date = 08/13/16 Pct Recovery = 106% Analysis Date = 08/08/16 Pct Recovery = 106% Analysis Date = 08/08/16 Pct Recovery = 106% Analysis Date = 08/03/16 Pct Recovery = 106% Analysis Date = 08/03/16 Pct Recovery = 106% Analysis Date = 07/29/16 Pct Recovery = 106% Analysis Date = 07/29/16 Pct Recovery = 106% Analysis Date = 07/24/16 Pct Recovery = 106% Analysis Date = 07/24/16 Pct Recovery = 106% Analysis Date = 07/20/16 Pct Recovery = 106% Analysis Date = 07/20/16 Pct Recovery = 106% Analysis Date = 07/15/16 Pct Recovery = 106% Analysis Date = 07/15/16 Pct Recovery = 106% Analysis Date = 07/10/16 Pct Recovery = 106% Analysis Date = 07/10/16 Pct Recovery = 106% Analysis Date = 07/05/16 Pct Recovery = 106% Analysis Date = 07/05/16 Pct Recovery = 106% Analysis Date = 06/30/16 Pct Recovery = 106% Analysis Date = 06/30/16 Pct Recovery = 106% Analysis Date = 06/26/16 Pct Recovery = 106% Analysis Date = 06/26/16 Pct Recovery = 106% Analysis Date = 06/21/16 Pct Recovery = 106% Analysis Date = 06/21/16 Pct Recovery = 106% Analysis Date = 06/16/16 Pct Recovery = 106% Analysis Date = 06/16/16 Pct Recovery = 106% Analysis Date = 06/11/16 Pct Recovery = 106% Analysis Date = 06/11/16 Pct Recovery = 106% Analysis Date = 06/06/16 Pct Recovery = 106% Analysis Date = 06/06/16 Pct Recovery = 106% Analysis Date = 06/02/16 Pct Recovery = 106% Analysis Date = 06/02/16 Pct Recovery = 106% Analysis Date = 05/28/16 Pct Recovery = 106% Analysis Date = 05/28/16 Pct Recovery = 106% Analysis Date = 05/23/16 Pct Recovery = 106% Analysis Date = 05/23/16 Pct Recovery = 106% Analysis Date = 05/18/16 Pct Recovery = 106% Analysis Date = 05/18/16 Pct Recovery = 106% Analysis Date = 05/13/16 Pct Recovery = 106% Analysis Date = 05/13/16 Pct Recovery = 106% Analysis Date = 05/09/16 Pct Recovery = 106% Analysis Date = 05/09/16 Pct Recovery = 106% Analysis Date = 05/04/16 Pct Recovery = 107% Analysis Date = 05/04/16 Pct Recovery = 107% Analysis Date = 04/29/16 Pct Recovery = 107% Analysis Date = 04/29/16 Pct Recovery = 107% Analysis Date = 04/24/16 Pct Recovery = 107% Analysis Date = 04/24/16 Pct Recovery = 107% Analysis Date = 04/19/16 Pct Recovery = 107% Analysis Date = 04/19/16 Pct Recovery = 107% Analysis Date = 04/15/16 Pct Recovery = 107% Analysis Date = 04/15/16 Pct Recovery = 107% Analysis Date = 04/10/16 Pct Recovery = 107% Analysis Date = 04/10/16 Pct Recovery = 107% Analysis Date = 04/05/16 Pct Recovery = 107% Analysis Date = 04/05/16 Pct Recovery = 107% Analysis Date = 03/31/16 Pct Recovery = 107% Analysis Date = 03/31/16 Pct Recovery = 107% Analysis Date = 03/26/16 Pct Recovery = 107% Analysis Date = 03/26/16 Pct Recovery = 107% Analysis Date = 03/22/16 Pct Recovery = 107% Analysis Date = 03/22/16 Pct Recovery = 107% Analysis Date = 03/17/16 Pct Recovery = 107% Analysis Date = 03/17/16 Pct Recovery = 107% Analysis Date = 03/12/16 Pct Recovery = 107% Analysis Date = 03/12/16 Pct Recovery = 107% Analysis Date = 03/07/16 Pct Recovery = 107% Analysis Date = 03/07/16 Pct Recovery = 107% Analysis Date = 03/02/16 Pct Recovery = 107% Analysis Date = 03/02/16 Pct Recovery = 107% Analysis Date = 02/27/16 Pct Recovery = 107% Analysis Date = 02/27/16 Pct Recovery = 107% Analysis Date = 02/22/16 Pct Recovery = 107% Analysis Date = 02/22/16 Pct Recovery = 107% Analysis Date = 02/17/16 Pct Recovery = 107% Analysis Date = 02/17/16 Pct Recovery = 107% Analysis Date = 02/12/16 Pct Recovery = 107% Analysis Date = 02/12/16 Pct Recovery = 107% Analysis Date = 02/07/16 Pct Recovery = 107% Analysis Date = 02/07/16 Pct Recovery = 107% Analysis Date = 02/03/16 Pct Recovery = 107% Analysis Date = 02/03/16 Pct Recovery = 107% Analysis Date = 01/29/16 Pct Recovery = 107% Analysis Date = 01/29/16 Pct Recovery = 107% Analysis Date = 01/24/16 Pct Recovery = 107% Analysis Date = 01/24/16 Pct Recovery = 107% Analysis Date = 01/19/16 Pct Recovery = 107% Analysis Date = 01/19/16 Pct Recovery = 107% Analysis Date = 01/14/16 Pct Recovery = 107% Analysis Date = 01/14/16 Pct Recovery = 107% Analysis Date = 01/10/16 Pct Recovery = 107% Analysis Date = 01/10/16 Pct Recovery = 107% Analysis Date = 01/05/16 Pct Recovery = 107% Analysis Date = 01/05/16 Pct Recovery = 107% Analysis Date = 12/31/15 Pct Recovery = 107% Analysis Date = 12/31/15 Pct Recovery = 107% Analysis Date = 12/26/15 Pct Recovery = 107% Analysis Date = 12/26/15 Pct Recovery = 107% Analysis Date = 12/21/15 Pct Recovery = 107% Analysis Date = 12/21/15 Pct Recovery = 107% Analysis Date = 12/17/15 Pct Recovery = 107% Analysis Date = 12/17/15 Pct Recovery = 107% Analysis Date = 12/12/15 Pct Recovery = 107% Analysis Date = 12/12/15 Pct Recovery = 107% Analysis Date = 12/07/15 Pct Recovery = 107% Analysis Date = 12/07/15 Pct Recovery = 107% Analysis Date = 12/02/15 Pct Recovery = 107% Analysis Date = 12/02/15 Pct Recovery = 107% Analysis Date = 11/27/15 Pct Recovery = 107% Analysis Date = 11/27/15 Pct Recovery = 107% Analysis Date = 11/23/15 Pct Recovery = 106% Analysis Date = 11/23/15 Pct Recovery = 106% Analysis Date = 11/18/15 Pct Recovery = 106% Analysis Date = 11/18/15 Pct Recovery = 106% Analysis Date = 11/13/15 Pct Recovery = 106% Analysis Date = 11/13/15 Pct Recovery = 106% Analysis Date = 11/08/15 Pct Recovery = 106% Analysis Date = 11/08/15 Pct Recovery = 106% Analysis Date = 11/03/15 Pct Recovery = 106% Analysis Date = 11/03/15 Pct Recovery = 106% Analysis Date = 10/30/15 Pct Recovery = 106% Analysis Date = 10/30/15 Pct Recovery = 106% Analysis Date = 10/25/15 Pct Recovery = 106% Analysis Date = 10/25/15 Pct Recovery = 106% Analysis Date = 10/20/15 Pct Recovery = 106% Analysis Date = 10/20/15 Pct Recovery = 106% Analysis Date = 10/15/15 Pct Recovery = 106% Analysis Date = 10/15/15 Pct Recovery = 106% Analysis Date = 10/10/15 Pct Recovery = 106% Analysis Date = 10/10/15 Pct Recovery = 106% Analysis Date = 10/06/15 Pct Recovery = 105% Analysis Date = 10/06/15 Pct Recovery = 105% Analysis Date = 10/01/15 Pct Recovery = 105% Analysis Date = 10/01/15 Pct Recovery = 105% Analysis Date = 09/26/15 Pct Recovery = 105% Analysis Date = 09/26/15 Pct Recovery = 105% Analysis Date = 09/21/15 Pct Recovery = 105% Analysis Date = 09/21/15 Pct Recovery = 105% Analysis Date = 09/16/15 Pct Recovery = 105% Analysis Date = 09/16/15 Pct Recovery = 105% Analysis Date = 09/12/15 Pct Recovery = 105% Analysis Date = 09/12/15 Pct Recovery = 105% Analysis Date = 09/07/15 Pct Recovery = 105% Analysis Date = 09/07/15 Pct Recovery = 105% Analysis Date = 09/02/15 Pct Recovery = 105% Analysis Date = 09/02/15 Pct Recovery = 105% Analysis Date = 08/28/15 Pct Recovery = 104% Analysis Date = 08/28/15 Pct Recovery = 104% Analysis Date = 08/23/15 Pct Recovery = 104% Analysis Date = 08/23/15 Pct Recovery = 104% Analysis Date = 08/19/15 Pct Recovery = 104% Analysis Date = 08/19/15 Pct Recovery = 104% Analysis Date = 08/14/15 Pct Recovery = 104% Analysis Date = 08/14/15 Pct Recovery = 104% Analysis Date = 08/09/15 Pct Recovery = 104% Analysis Date = 08/09/15 Pct Recovery = 104% Analysis Date = 08/04/15 Pct Recovery = 104% Analysis Date = 08/04/15 Pct Recovery = 104% Analysis Date = 07/30/15 Pct Recovery = 104% Analysis Date = 07/30/15 Pct Recovery = 104% Analysis Date = 07/26/15 Pct Recovery = 103% Analysis Date = 07/26/15 Pct Recovery = 103% Analysis Date = 07/21/15 Pct Recovery = 103% Analysis Date = 07/21/15 Pct Recovery = 103% Analysis Date = 07/16/15 Pct Recovery = 103% Analysis Date = 07/16/15 Pct Recovery = 103% Analysis Date = 07/11/15 Pct Recovery = 103% Analysis Date = 07/11/15 Pct Recovery = 103% Analysis Date = 07/06/15 Pct Recovery = 103% Analysis Date = 07/06/15 Pct Recovery = 103% Analysis Date = 07/02/15 Pct Recovery = 103% Analysis Date = 07/02/15 Pct Recovery = 103% Analysis Date = 06/27/15 Pct Recovery = 103% Analysis Date = 06/27/15 Pct Recovery = 103% Analysis Date = 06/22/15 Pct Recovery = 103% Analysis Date = 06/22/15 Pct Recovery = 103% Analysis Date = 06/17/15 Pct Recovery = 102% Analysis Date = 06/17/15 Pct Recovery = 102% Analysis Date = 06/12/15 Pct Recovery = 102% Analysis Date = 06/12/15 Pct Recovery = 102% Analysis Date = 06/08/15 Pct Recovery = 102% Analysis Date = 06/08/15 Pct Recovery = 102% Analysis Date = 06/03/15 Pct Recovery = 102% Analysis Date = 06/03/15 Pct Recovery = 102% Analysis Date = 05/29/15 Pct Recovery = 102% Analysis Date = 05/29/15 Pct Recovery = 102% Analysis Date = 05/24/15 Pct Recovery = 102% Analysis Date = 05/24/15 Pct Recovery = 102% Analysis Date = 05/19/15 Pct Recovery = 102% Analysis Date = 05/19/15 Pct Recovery = 102% Analysis Date = 05/15/15 Pct Recovery = 102% Analysis Date = 05/15/15 Pct Recovery = 102% Analysis Date = 05/10/15 Pct Recovery = 101% Analysis Date = 05/10/15 Pct Recovery = 101% Analysis Date = 05/05/15 Pct Recovery = 101% Analysis Date = 05/05/15 Pct Recovery = 101% Analysis Date = 04/30/15 Pct Recovery = 101% Analysis Date = 04/30/15 Pct Recovery = 101% Analysis Date = 04/25/15 Pct Recovery = 101% Analysis Date = 04/25/15 Pct Recovery = 101% Analysis Date = 04/21/15 Pct Recovery = 101% Analysis Date = 04/21/15 Pct Recovery = 101% Analysis Date = 04/16/15 Pct Recovery = 101% Analysis Date = 04/16/15 Pct Recovery = 101% Analysis Date = 04/11/15 Pct Recovery = 101% Analysis Date = 04/11/15 Pct Recovery = 101% Analysis Date = 04/06/15 Pct Recovery = 101% Analysis Date = 04/06/15 Pct Recovery = 101% Analysis Date = 04/01/15 Pct Recovery = 101% Analysis Date = 04/01/15 Pct Recovery = 101% Analysis Date = 03/28/15 Pct Recovery = 101% Analysis Date = 03/28/15 Pct Recovery = 101% Analysis Date = 03/23/15 Pct Recovery = 101% Analysis Date = 03/23/15 Pct Recovery = 101% Analysis Date = 03/18/15 Pct Recovery = 101% Analysis Date = 03/18/15 Pct Recovery = 101% Analysis Date = 03/13/15 Pct Recovery = 100% Analysis Date = 03/13/15 Pct Recovery = 100% Analysis Date = 03/08/15 Pct Recovery = 100% Analysis Date = 03/08/15 Pct Recovery = 100% Analysis Date = 03/04/15 Pct Recovery = 100% Analysis Date = 03/04/15 Pct Recovery = 100% Analysis Date = 02/27/15 Pct Recovery = 100% Analysis Date = 02/27/15 Pct Recovery = 100% Analysis Date = 02/22/15 Pct Recovery = 101% Analysis Date = 02/22/15 Pct Recovery = 101% Analysis Date = 02/17/15 Pct Recovery = 101% Analysis Date = 02/17/15 Pct Recovery = 101% Analysis Date = 02/12/15 Pct Recovery = 101% Analysis Date = 02/12/15 Pct Recovery = 101% Analysis Date = 02/08/15 Pct Recovery = 101% Analysis Date = 02/08/15 Pct Recovery = 101% Analysis Date = 02/03/15 Pct Recovery = 101% Analysis Date = 02/03/15 Pct Recovery = 101% Analysis Date = 01/29/15 Pct Recovery = 101% Analysis Date = 01/29/15 Pct Recovery = 101% Analysis Date = 01/24/15 Pct Recovery = 101% Analysis Date = 01/24/15 Pct Recovery = 101% Analysis Date = 01/19/15 Pct Recovery = 101% Analysis Date = 01/19/15 Pct Recovery = 101% Analysis Date = 01/15/15 Pct Recovery = 101% Analysis Date = 01/15/15 Pct Recovery = 101% Analysis Date = 01/10/15 Pct Recovery = 102% Analysis Date = 01/10/15 Pct Recovery = 102% Analysis Date = 01/05/15 Pct Recovery = 102% Analysis Date = 01/05/15 Pct Recovery = 102% Analysis Date = 12/31/14 Pct Recovery = 102% Analysis Date = 12/31/14 Pct Recovery = 102% Analysis Date = 12/26/14 Pct Recovery = 102% Analysis Date = 12/26/14 Pct Recovery = 102% Analysis Date = 12/22/14 Pct Recovery = 102% Analysis Date = 12/22/14 Pct Recovery = 102% Analysis Date = 12/17/14 Pct Recovery = 102% Analysis Date = 12/17/14 Pct Recovery = 102% Analysis Date = 12/12/14 Pct Recovery = 102% Analysis Date = 12/12/14 Pct Recovery = 102% Analysis Date = 12/07/14 Pct Recovery = 102% Analysis Date = 12/07/14 Pct Recovery = 102% Analysis Date = 12/02/14 Pct Recovery = 102% Analysis Date = 12/02/14 Pct Recovery = 102% Analysis Date = 11/28/14 Pct Recovery = 102% Analysis Date = 11/28/14 Pct Recovery = 102% Analysis Date = 11/23/14 Pct Recovery = 103% Analysis Date = 11/23/14 Pct Recovery = 103% Analysis Date = 11/18/14 Pct Recovery = 103% Analysis Date = 11/18/14 Pct Recovery = 103% Analysis Date = 11/13/14 Pct Recovery = 103% Analysis Date = 11/13/14 Pct Recovery = 103% Analysis Date = 11/08/14 Pct Recovery = 103% Analysis Date = 11/08/14 Pct Recovery = 103% Analysis Date = 11/04/14 Pct Recovery = 103% Analysis Date = 11/04/14 Pct Recovery = 103% Analysis Date = 10/30/14 Pct Recovery = 103% Analysis Date = 10/30/14 Pct Recovery = 103% Analysis Date = 10/25/14 Pct Recovery = 103% Analysis Date = 10/25/14 Pct Recovery = 103% Analysis Date = 10/20/14 Pct Recovery = 103% Analysis Date = 10/20/14 Pct Recovery = 103% Analysis Date = 10/15/14 Pct Recovery = 104% Analysis Date = 10/15/14 Pct Recovery = 104% Analysis Date = 10/11/14 Pct Recovery = 104% Analysis Date = 10/11/14 Pct Recovery = 104% Analysis Date = 10/06/14 Pct Recovery = 104% Analysis Date = 10/06/14 Pct Recovery = 104% Analysis Date = 10/01/14 Pct Recovery = 104% Analysis Date = 10/01/14 Pct Recovery = 104% Analysis Date = 09/26/14 Pct Recovery = 104% Analysis Date = 09/26/14 Pct Recovery = 104% Analysis Date = 09/21/14 Pct Recovery = 104% Analysis Date = 09/21/14 Pct Recovery = 104% Analysis Date = 09/17/14 Pct Recovery = 104% Analysis Date = 09/17/14 Pct Recovery = 104% Analysis Date = 09/12/14 Pct Recovery = 105% Analysis Date = 09/12/14 Pct Recovery = 105% Analysis Date = 09/07/14 Pct Recovery = 105% Analysis Date = 09/07/14 Pct Recovery = 105% Analysis Date = 09/02/14 Pct Recovery = 105% Analysis Date = 09/02/14 Pct Recovery = 105% Analysis Date = 08/28/14 Pct Recovery = 105% Analysis Date = 08/28/14 Pct Recovery = 105% Analysis Date = 08/24/14 Pct Recovery = 105% Analysis Date = 08/24/14 Pct Recovery = 105% Analysis Date = 08/19/14 Pct Recovery = 105% Analysis Date = 08/19/14 Pct Recovery = 105% Analysis Date = 08/14/14 Pct Recovery = 106% Analysis Date = 08/14/14 Pct Recovery = 106% Analysis Date = 08/09/14 Pct Recovery = 106% Analysis Date = 08/09/14 Pct Recovery = 106% Analysis Date = 08/04/14 Pct Recovery = 106% Analysis Date = 08/04/14 Pct Recovery = 106% Analysis Date = 07/31/14 Pct Recovery = 106% Analysis Date = 07/31/14 Pct Recovery = 106% Analysis Date = 07/26/14 Pct Recovery = 106% Analysis Date = 07/26/14 Pct Recovery = 106% Analysis Date = 07/21/14 Pct Recovery = 106% Analysis Date = 07/21/14 Pct Recovery = 106% Analysis Date = 07/16/14 Pct Recovery = 107% Analysis Date = 07/16/14 Pct Recovery = 107% Analysis Date = 07/11/14 Pct Recovery = 107% Analysis Date = 07/11/14 Pct Recovery = 107% Analysis Date = 07/07/14 Pct Recovery = 107% Analysis Date = 07/07/14 Pct Recovery = 107% Analysis Date = 07/02/14 Pct Recovery = 107% Analysis Date = 07/02/14 Pct Recovery = 107% Analysis Date = 06/27/14 Pct Recovery = 107% Analysis Date = 06/27/14 Pct Recovery = 107% Analysis Date = 06/22/14 Pct Recovery = 107% Analysis Date = 06/22/14 Pct Recovery = 107% Analysis Date = 06/17/14 Pct Recovery = 108% Analysis Date = 06/17/14 Pct Recovery = 108% Analysis Date = 06/13/14 Pct Recovery = 108% Analysis Date = 06/13/14 Pct Recovery = 108% Analysis Date = 06/08/14 Pct Recovery = 108% Analysis Date = 06/08/14 Pct Recovery = 108% Analysis Date = 06/03/14 Pct Recovery = 108% Analysis Date = 06/03/14 Pct Recovery = 108% Analysis Date = 05/29/14 Pct Recovery = 108% Analysis Date = 05/29/14 Pct Recovery = 108% Analysis Date = 05/24/14 Pct Recovery = 109% Analysis Date = 05/24/14 Pct Recovery = 109% Analysis Date = 05/20/14 Pct Recovery = 109% Analysis Date = 05/20/14 Pct Recovery = 109% Analysis Date = 05/15/14 Pct Recovery = 109% Analysis Date = 05/15/14 Pct Recovery = 109% Analysis Date = 05/10/14 Pct Recovery = 109% Analysis Date = 05/10/14 Pct Recovery = 109% Analysis Date = 05/05/14 Pct Recovery = 109% Analysis Date = 05/05/14 Pct Recovery = 109% Analysis Date = 05/01/14 Pct Recovery = 110% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
BROMODICHLOROMETHANE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 49 105% 10% 103% 8%
Total 49 105% 10% 103% 8%

Sample Statistics
BROMODICHLOROMETHANE

Characteristic N % % Basis
Plotted 49 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 49 .  
False Negatives 0 0% 0 out of 49
Not Spiked 24 .  
False Positives 1 4% 1 out of 24

BQS OBSP Determination:
BROMOETHENE
METHOD: 4440 , TESTIDCODE: 50002GCM66
Open Data Set

Analysis Date = 12/12/16 SpikeMix = Accu 216041125: 40 µl & Crescent 03FF058: 40 µl Pct Recovery = 96% Analysis Date = 07/20/16 SpikeMix = Supelco LC20141V: 40 µl & Accu 216041125: 40 µl Pct Recovery = 101% Analysis Date = 07/14/16 SpikeMix = Accu 216041125: 40 µl & NSI 041816AVOC: 40 µl Pct Recovery = 98% Analysis Date = 09/08/16 SpikeMix = Supelco LC20141V: 25 µl & Accu 216041125: 25 µl Pct Recovery = 78% Analysis Date = 05/24/16 SpikeMix = Accu 216041125: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 97% Analysis Date = 03/19/15 SpikeMix = Spex Organics C1140417015: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 107% Analysis Date = 03/06/15 SpikeMix = ERA 0227-14-06.1A: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 70% Analysis Date = 12/17/14 SpikeMix = Supelco LC06438: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 92% Analysis Date = 11/22/14 SpikeMix = NSI 032614: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 98% Analysis Date = 09/21/14 SpikeMix = Supelco LC06438: 20 µl Pct Recovery = 100% Analysis Date = 08/19/14 SpikeMix = Spex Organics C1140417015: 20 µl & Accu 214031115: 20 µl Pct Recovery = 130% Analysis Date = 08/16/14 SpikeMix = ERA 0227-14-06.1A: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 122% Analysis Date = 06/10/14 SpikeMix = NSI 032614: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 110% Analysis Date = 08/15/15 SpikeMix = Supelco LC13545: 25 µl & Crescent 04EE008: 25 µl Pct Recovery = 94% Analysis Date = 07/13/15 SpikeMix = Crescent 04EE008: 25 µl & NSI 050515AVOC: 25 µl Pct Recovery = 99% Analysis Date = 09/29/15 SpikeMix = Accu 215041380: 25 µl & ERA 0406-15-03: 25 µl Pct Recovery = 92% Analysis Date = 10/13/16 SpikeMix = Accu 216041125: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 105% Analysis Date = 08/20/16 SpikeMix = Accu 216041125: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 106% Analysis Date = 06/30/16 SpikeMix = ChemService 5082900: 15 µl & Accu 216041125: 15 µl Pct Recovery = 67% Analysis Date = 12/18/15 SpikeMix = Supelco LC13545: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 88% Analysis Date = 10/17/15 SpikeMix = Crescent 04EE008: 15 µl & NSI 050515AVOC: 15 µl Pct Recovery = 80% Analysis Date = 05/09/15 SpikeMix = Spex Organics EN150428007: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 91% Analysis Date = 04/02/16 SpikeMix = Supelco LC13545: 15 µl & Accu 215041380: 15 µl Pct Recovery = 110% Analysis Date = 03/04/16 SpikeMix = Accu 215041380: 15 µl & ERA 0406-15-03: 15 µl Pct Recovery = 98% Analysis Date = 06/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Accu 215041380: 15 µl Pct Recovery = 94% Analysis Date = 11/06/14 SpikeMix = Spex Organics C1140417015: 10 µl & Crescent 03DD004: 10 µl Pct Recovery = 76% Analysis Date = 10/21/14 SpikeMix = ERA 0227-14-06.1A: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 89% Analysis Date = 09/09/14 SpikeMix = NSI 032614: 10 µl & Spex Organics C1140417015: 10 µl Pct Recovery = 142% Analysis Date = 07/23/14 SpikeMix = Spex Organics C1140417015: 10 µl & Accu 214031115: 10 µl Pct Recovery = 128% Analysis Date = 07/11/14 SpikeMix = Spex Organics C1140417015: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 74% Analysis Date = 06/18/14 SpikeMix = Supelco LC06438: 10 µl & Accu 214031115: 10 µl Pct Recovery = 108% Analysis Date = 05/30/14 SpikeMix = NSI 032614: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 122% Analysis Date = 05/03/14 SpikeMix = Crescent 03DD004: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 100% Analysis Date = 05/13/16 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 89% Analysis Date = 01/27/16 SpikeMix = Crescent 04EE008: 10 µl & NSI 050515AVOC: 10 µl Pct Recovery = 101% Analysis Date = 07/31/15 SpikeMix = Crescent 04EE008: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 79% Analysis Date = 05/09/15 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 96% Analysis Date = 02/18/16 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 104% Analysis Date = 11/20/15 SpikeMix = Accu 215041380: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 100% Analysis Date = 11/12/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 93% Analysis Date = 05/21/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 94% Analysis Date = 12/12/16 Pct Recovery = 95% Analysis Date = 12/07/16 Pct Recovery = 95% Analysis Date = 12/07/16 Pct Recovery = 95% Analysis Date = 12/02/16 Pct Recovery = 95% Analysis Date = 12/02/16 Pct Recovery = 95% Analysis Date = 11/27/16 Pct Recovery = 95% Analysis Date = 11/27/16 Pct Recovery = 95% Analysis Date = 11/22/16 Pct Recovery = 95% Analysis Date = 11/22/16 Pct Recovery = 95% Analysis Date = 11/18/16 Pct Recovery = 95% Analysis Date = 11/18/16 Pct Recovery = 95% Analysis Date = 11/13/16 Pct Recovery = 95% Analysis Date = 11/13/16 Pct Recovery = 95% Analysis Date = 11/08/16 Pct Recovery = 95% Analysis Date = 11/08/16 Pct Recovery = 95% Analysis Date = 11/03/16 Pct Recovery = 95% Analysis Date = 11/03/16 Pct Recovery = 95% Analysis Date = 10/30/16 Pct Recovery = 95% Analysis Date = 10/30/16 Pct Recovery = 95% Analysis Date = 10/25/16 Pct Recovery = 95% Analysis Date = 10/25/16 Pct Recovery = 95% Analysis Date = 10/20/16 Pct Recovery = 95% Analysis Date = 10/20/16 Pct Recovery = 95% Analysis Date = 10/15/16 Pct Recovery = 95% Analysis Date = 10/15/16 Pct Recovery = 95% Analysis Date = 10/10/16 Pct Recovery = 95% Analysis Date = 10/10/16 Pct Recovery = 95% Analysis Date = 10/06/16 Pct Recovery = 95% Analysis Date = 10/06/16 Pct Recovery = 95% Analysis Date = 10/01/16 Pct Recovery = 95% Analysis Date = 10/01/16 Pct Recovery = 95% Analysis Date = 09/26/16 Pct Recovery = 95% Analysis Date = 09/26/16 Pct Recovery = 95% Analysis Date = 09/21/16 Pct Recovery = 95% Analysis Date = 09/21/16 Pct Recovery = 95% Analysis Date = 09/17/16 Pct Recovery = 95% Analysis Date = 09/17/16 Pct Recovery = 95% Analysis Date = 09/12/16 Pct Recovery = 95% Analysis Date = 09/12/16 Pct Recovery = 95% Analysis Date = 09/07/16 Pct Recovery = 95% Analysis Date = 09/07/16 Pct Recovery = 95% Analysis Date = 09/02/16 Pct Recovery = 95% Analysis Date = 09/02/16 Pct Recovery = 95% Analysis Date = 08/29/16 Pct Recovery = 95% Analysis Date = 08/29/16 Pct Recovery = 95% Analysis Date = 08/24/16 Pct Recovery = 95% Analysis Date = 08/24/16 Pct Recovery = 95% Analysis Date = 08/19/16 Pct Recovery = 95% Analysis Date = 08/19/16 Pct Recovery = 95% Analysis Date = 08/14/16 Pct Recovery = 95% Analysis Date = 08/14/16 Pct Recovery = 95% Analysis Date = 08/09/16 Pct Recovery = 95% Analysis Date = 08/09/16 Pct Recovery = 95% Analysis Date = 08/05/16 Pct Recovery = 95% Analysis Date = 08/05/16 Pct Recovery = 95% Analysis Date = 07/31/16 Pct Recovery = 95% Analysis Date = 07/31/16 Pct Recovery = 95% Analysis Date = 07/26/16 Pct Recovery = 95% Analysis Date = 07/26/16 Pct Recovery = 95% Analysis Date = 07/21/16 Pct Recovery = 95% Analysis Date = 07/21/16 Pct Recovery = 95% Analysis Date = 07/17/16 Pct Recovery = 95% Analysis Date = 07/17/16 Pct Recovery = 95% Analysis Date = 07/12/16 Pct Recovery = 95% Analysis Date = 07/12/16 Pct Recovery = 95% Analysis Date = 07/07/16 Pct Recovery = 95% Analysis Date = 07/07/16 Pct Recovery = 95% Analysis Date = 07/02/16 Pct Recovery = 95% Analysis Date = 07/02/16 Pct Recovery = 95% Analysis Date = 06/28/16 Pct Recovery = 95% Analysis Date = 06/28/16 Pct Recovery = 95% Analysis Date = 06/23/16 Pct Recovery = 95% Analysis Date = 06/23/16 Pct Recovery = 95% Analysis Date = 06/18/16 Pct Recovery = 95% Analysis Date = 06/18/16 Pct Recovery = 95% Analysis Date = 06/13/16 Pct Recovery = 95% Analysis Date = 06/13/16 Pct Recovery = 95% Analysis Date = 06/08/16 Pct Recovery = 95% Analysis Date = 06/08/16 Pct Recovery = 95% Analysis Date = 06/04/16 Pct Recovery = 95% Analysis Date = 06/04/16 Pct Recovery = 95% Analysis Date = 05/30/16 Pct Recovery = 95% Analysis Date = 05/30/16 Pct Recovery = 95% Analysis Date = 05/25/16 Pct Recovery = 95% Analysis Date = 05/25/16 Pct Recovery = 95% Analysis Date = 05/20/16 Pct Recovery = 95% Analysis Date = 05/20/16 Pct Recovery = 95% Analysis Date = 05/16/16 Pct Recovery = 95% Analysis Date = 05/16/16 Pct Recovery = 95% Analysis Date = 05/11/16 Pct Recovery = 95% Analysis Date = 05/11/16 Pct Recovery = 95% Analysis Date = 05/06/16 Pct Recovery = 95% Analysis Date = 05/06/16 Pct Recovery = 95% Analysis Date = 05/01/16 Pct Recovery = 95% Analysis Date = 05/01/16 Pct Recovery = 95% Analysis Date = 04/27/16 Pct Recovery = 95% Analysis Date = 04/27/16 Pct Recovery = 95% Analysis Date = 04/22/16 Pct Recovery = 95% Analysis Date = 04/22/16 Pct Recovery = 95% Analysis Date = 04/17/16 Pct Recovery = 95% Analysis Date = 04/17/16 Pct Recovery = 95% Analysis Date = 04/12/16 Pct Recovery = 95% Analysis Date = 04/12/16 Pct Recovery = 95% Analysis Date = 04/07/16 Pct Recovery = 95% Analysis Date = 04/07/16 Pct Recovery = 95% Analysis Date = 04/03/16 Pct Recovery = 95% Analysis Date = 04/03/16 Pct Recovery = 95% Analysis Date = 03/29/16 Pct Recovery = 95% Analysis Date = 03/29/16 Pct Recovery = 95% Analysis Date = 03/24/16 Pct Recovery = 95% Analysis Date = 03/24/16 Pct Recovery = 95% Analysis Date = 03/19/16 Pct Recovery = 95% Analysis Date = 03/19/16 Pct Recovery = 95% Analysis Date = 03/15/16 Pct Recovery = 95% Analysis Date = 03/15/16 Pct Recovery = 95% Analysis Date = 03/10/16 Pct Recovery = 95% Analysis Date = 03/10/16 Pct Recovery = 95% Analysis Date = 03/05/16 Pct Recovery = 94% Analysis Date = 03/05/16 Pct Recovery = 94% Analysis Date = 02/29/16 Pct Recovery = 95% Analysis Date = 02/29/16 Pct Recovery = 95% Analysis Date = 02/25/16 Pct Recovery = 95% Analysis Date = 02/25/16 Pct Recovery = 95% Analysis Date = 02/20/16 Pct Recovery = 95% Analysis Date = 02/20/16 Pct Recovery = 95% Analysis Date = 02/15/16 Pct Recovery = 95% Analysis Date = 02/15/16 Pct Recovery = 95% Analysis Date = 02/10/16 Pct Recovery = 95% Analysis Date = 02/10/16 Pct Recovery = 95% Analysis Date = 02/05/16 Pct Recovery = 95% Analysis Date = 02/05/16 Pct Recovery = 95% Analysis Date = 02/01/16 Pct Recovery = 95% Analysis Date = 02/01/16 Pct Recovery = 95% Analysis Date = 01/27/16 Pct Recovery = 95% Analysis Date = 01/27/16 Pct Recovery = 95% Analysis Date = 01/22/16 Pct Recovery = 95% Analysis Date = 01/22/16 Pct Recovery = 95% Analysis Date = 01/17/16 Pct Recovery = 95% Analysis Date = 01/17/16 Pct Recovery = 95% Analysis Date = 01/13/16 Pct Recovery = 95% Analysis Date = 01/13/16 Pct Recovery = 95% Analysis Date = 01/08/16 Pct Recovery = 95% Analysis Date = 01/08/16 Pct Recovery = 95% Analysis Date = 01/03/16 Pct Recovery = 94% Analysis Date = 01/03/16 Pct Recovery = 94% Analysis Date = 12/29/15 Pct Recovery = 94% Analysis Date = 12/29/15 Pct Recovery = 94% Analysis Date = 12/25/15 Pct Recovery = 94% Analysis Date = 12/25/15 Pct Recovery = 94% Analysis Date = 12/20/15 Pct Recovery = 94% Analysis Date = 12/20/15 Pct Recovery = 94% Analysis Date = 12/15/15 Pct Recovery = 94% Analysis Date = 12/15/15 Pct Recovery = 94% Analysis Date = 12/10/15 Pct Recovery = 94% Analysis Date = 12/10/15 Pct Recovery = 94% Analysis Date = 12/05/15 Pct Recovery = 94% Analysis Date = 12/05/15 Pct Recovery = 94% Analysis Date = 12/01/15 Pct Recovery = 94% Analysis Date = 12/01/15 Pct Recovery = 94% Analysis Date = 11/26/15 Pct Recovery = 94% Analysis Date = 11/26/15 Pct Recovery = 94% Analysis Date = 11/21/15 Pct Recovery = 94% Analysis Date = 11/21/15 Pct Recovery = 94% Analysis Date = 11/16/15 Pct Recovery = 94% Analysis Date = 11/16/15 Pct Recovery = 94% Analysis Date = 11/12/15 Pct Recovery = 94% Analysis Date = 11/12/15 Pct Recovery = 94% Analysis Date = 11/07/15 Pct Recovery = 94% Analysis Date = 11/07/15 Pct Recovery = 94% Analysis Date = 11/02/15 Pct Recovery = 94% Analysis Date = 11/02/15 Pct Recovery = 94% Analysis Date = 10/28/15 Pct Recovery = 94% Analysis Date = 10/28/15 Pct Recovery = 94% Analysis Date = 10/24/15 Pct Recovery = 94% Analysis Date = 10/24/15 Pct Recovery = 94% Analysis Date = 10/19/15 Pct Recovery = 94% Analysis Date = 10/19/15 Pct Recovery = 94% Analysis Date = 10/14/15 Pct Recovery = 94% Analysis Date = 10/14/15 Pct Recovery = 94% Analysis Date = 10/09/15 Pct Recovery = 94% Analysis Date = 10/09/15 Pct Recovery = 94% Analysis Date = 10/04/15 Pct Recovery = 94% Analysis Date = 10/04/15 Pct Recovery = 94% Analysis Date = 09/30/15 Pct Recovery = 94% Analysis Date = 09/30/15 Pct Recovery = 94% Analysis Date = 09/25/15 Pct Recovery = 94% Analysis Date = 09/25/15 Pct Recovery = 94% Analysis Date = 09/20/15 Pct Recovery = 93% Analysis Date = 09/20/15 Pct Recovery = 93% Analysis Date = 09/15/15 Pct Recovery = 93% Analysis Date = 09/15/15 Pct Recovery = 93% Analysis Date = 09/11/15 Pct Recovery = 93% Analysis Date = 09/11/15 Pct Recovery = 93% Analysis Date = 09/06/15 Pct Recovery = 93% Analysis Date = 09/06/15 Pct Recovery = 93% Analysis Date = 09/01/15 Pct Recovery = 93% Analysis Date = 09/01/15 Pct Recovery = 93% Analysis Date = 08/27/15 Pct Recovery = 93% Analysis Date = 08/27/15 Pct Recovery = 93% Analysis Date = 08/23/15 Pct Recovery = 93% Analysis Date = 08/23/15 Pct Recovery = 93% Analysis Date = 08/18/15 Pct Recovery = 93% Analysis Date = 08/18/15 Pct Recovery = 93% Analysis Date = 08/13/15 Pct Recovery = 93% Analysis Date = 08/13/15 Pct Recovery = 93% Analysis Date = 08/08/15 Pct Recovery = 92% Analysis Date = 08/08/15 Pct Recovery = 92% Analysis Date = 08/03/15 Pct Recovery = 92% Analysis Date = 08/03/15 Pct Recovery = 92% Analysis Date = 07/30/15 Pct Recovery = 92% Analysis Date = 07/30/15 Pct Recovery = 92% Analysis Date = 07/25/15 Pct Recovery = 92% Analysis Date = 07/25/15 Pct Recovery = 92% Analysis Date = 07/20/15 Pct Recovery = 92% Analysis Date = 07/20/15 Pct Recovery = 92% Analysis Date = 07/15/15 Pct Recovery = 92% Analysis Date = 07/15/15 Pct Recovery = 92% Analysis Date = 07/11/15 Pct Recovery = 92% Analysis Date = 07/11/15 Pct Recovery = 92% Analysis Date = 07/06/15 Pct Recovery = 92% Analysis Date = 07/06/15 Pct Recovery = 92% Analysis Date = 07/01/15 Pct Recovery = 92% Analysis Date = 07/01/15 Pct Recovery = 92% Analysis Date = 06/26/15 Pct Recovery = 92% Analysis Date = 06/26/15 Pct Recovery = 92% Analysis Date = 06/21/15 Pct Recovery = 92% Analysis Date = 06/21/15 Pct Recovery = 92% Analysis Date = 06/17/15 Pct Recovery = 92% Analysis Date = 06/17/15 Pct Recovery = 92% Analysis Date = 06/12/15 Pct Recovery = 92% Analysis Date = 06/12/15 Pct Recovery = 92% Analysis Date = 06/07/15 Pct Recovery = 92% Analysis Date = 06/07/15 Pct Recovery = 92% Analysis Date = 06/02/15 Pct Recovery = 91% Analysis Date = 06/02/15 Pct Recovery = 91% Analysis Date = 05/29/15 Pct Recovery = 91% Analysis Date = 05/29/15 Pct Recovery = 91% Analysis Date = 05/24/15 Pct Recovery = 91% Analysis Date = 05/24/15 Pct Recovery = 91% Analysis Date = 05/19/15 Pct Recovery = 91% Analysis Date = 05/19/15 Pct Recovery = 91% Analysis Date = 05/14/15 Pct Recovery = 92% Analysis Date = 05/14/15 Pct Recovery = 92% Analysis Date = 05/10/15 Pct Recovery = 92% Analysis Date = 05/10/15 Pct Recovery = 92% Analysis Date = 05/05/15 Pct Recovery = 92% Analysis Date = 05/05/15 Pct Recovery = 92% Analysis Date = 04/30/15 Pct Recovery = 92% Analysis Date = 04/30/15 Pct Recovery = 92% Analysis Date = 04/25/15 Pct Recovery = 92% Analysis Date = 04/25/15 Pct Recovery = 92% Analysis Date = 04/20/15 Pct Recovery = 92% Analysis Date = 04/20/15 Pct Recovery = 92% Analysis Date = 04/16/15 Pct Recovery = 92% Analysis Date = 04/16/15 Pct Recovery = 92% Analysis Date = 04/11/15 Pct Recovery = 93% Analysis Date = 04/11/15 Pct Recovery = 93% Analysis Date = 04/06/15 Pct Recovery = 93% Analysis Date = 04/06/15 Pct Recovery = 93% Analysis Date = 04/01/15 Pct Recovery = 93% Analysis Date = 04/01/15 Pct Recovery = 93% Analysis Date = 03/28/15 Pct Recovery = 93% Analysis Date = 03/28/15 Pct Recovery = 93% Analysis Date = 03/23/15 Pct Recovery = 93% Analysis Date = 03/23/15 Pct Recovery = 93% Analysis Date = 03/18/15 Pct Recovery = 93% Analysis Date = 03/18/15 Pct Recovery = 93% Analysis Date = 03/13/15 Pct Recovery = 94% Analysis Date = 03/13/15 Pct Recovery = 94% Analysis Date = 03/09/15 Pct Recovery = 94% Analysis Date = 03/09/15 Pct Recovery = 94% Analysis Date = 03/04/15 Pct Recovery = 94% Analysis Date = 03/04/15 Pct Recovery = 94% Analysis Date = 02/27/15 Pct Recovery = 95% Analysis Date = 02/27/15 Pct Recovery = 95% Analysis Date = 02/22/15 Pct Recovery = 95% Analysis Date = 02/22/15 Pct Recovery = 95% Analysis Date = 02/17/15 Pct Recovery = 95% Analysis Date = 02/17/15 Pct Recovery = 95% Analysis Date = 02/13/15 Pct Recovery = 96% Analysis Date = 02/13/15 Pct Recovery = 96% Analysis Date = 02/08/15 Pct Recovery = 96% Analysis Date = 02/08/15 Pct Recovery = 96% Analysis Date = 02/03/15 Pct Recovery = 96% Analysis Date = 02/03/15 Pct Recovery = 96% Analysis Date = 01/29/15 Pct Recovery = 96% Analysis Date = 01/29/15 Pct Recovery = 96% Analysis Date = 01/25/15 Pct Recovery = 97% Analysis Date = 01/25/15 Pct Recovery = 97% Analysis Date = 01/20/15 Pct Recovery = 97% Analysis Date = 01/20/15 Pct Recovery = 97% Analysis Date = 01/15/15 Pct Recovery = 97% Analysis Date = 01/15/15 Pct Recovery = 97% Analysis Date = 01/10/15 Pct Recovery = 98% Analysis Date = 01/10/15 Pct Recovery = 98% Analysis Date = 01/06/15 Pct Recovery = 98% Analysis Date = 01/06/15 Pct Recovery = 98% Analysis Date = 01/01/15 Pct Recovery = 98% Analysis Date = 01/01/15 Pct Recovery = 98% Analysis Date = 12/27/14 Pct Recovery = 99% Analysis Date = 12/27/14 Pct Recovery = 99% Analysis Date = 12/22/14 Pct Recovery = 99% Analysis Date = 12/22/14 Pct Recovery = 99% Analysis Date = 12/17/14 Pct Recovery = 99% Analysis Date = 12/17/14 Pct Recovery = 99% Analysis Date = 12/13/14 Pct Recovery = 99% Analysis Date = 12/13/14 Pct Recovery = 99% Analysis Date = 12/08/14 Pct Recovery = 100% Analysis Date = 12/08/14 Pct Recovery = 100% Analysis Date = 12/03/14 Pct Recovery = 100% Analysis Date = 12/03/14 Pct Recovery = 100% Analysis Date = 11/28/14 Pct Recovery = 100% Analysis Date = 11/28/14 Pct Recovery = 100% Analysis Date = 11/24/14 Pct Recovery = 101% Analysis Date = 11/24/14 Pct Recovery = 101% Analysis Date = 11/19/14 Pct Recovery = 101% Analysis Date = 11/19/14 Pct Recovery = 101% Analysis Date = 11/14/14 Pct Recovery = 101% Analysis Date = 11/14/14 Pct Recovery = 101% Analysis Date = 11/09/14 Pct Recovery = 102% Analysis Date = 11/09/14 Pct Recovery = 102% Analysis Date = 11/05/14 Pct Recovery = 102% Analysis Date = 11/05/14 Pct Recovery = 102% Analysis Date = 10/31/14 Pct Recovery = 102% Analysis Date = 10/31/14 Pct Recovery = 102% Analysis Date = 10/26/14 Pct Recovery = 102% Analysis Date = 10/26/14 Pct Recovery = 102% Analysis Date = 10/21/14 Pct Recovery = 103% Analysis Date = 10/21/14 Pct Recovery = 103% Analysis Date = 10/16/14 Pct Recovery = 103% Analysis Date = 10/16/14 Pct Recovery = 103% Analysis Date = 10/12/14 Pct Recovery = 103% Analysis Date = 10/12/14 Pct Recovery = 103% Analysis Date = 10/07/14 Pct Recovery = 104% Analysis Date = 10/07/14 Pct Recovery = 104% Analysis Date = 10/02/14 Pct Recovery = 104% Analysis Date = 10/02/14 Pct Recovery = 104% Analysis Date = 09/27/14 Pct Recovery = 104% Analysis Date = 09/27/14 Pct Recovery = 104% Analysis Date = 09/23/14 Pct Recovery = 105% Analysis Date = 09/23/14 Pct Recovery = 105% Analysis Date = 09/18/14 Pct Recovery = 105% Analysis Date = 09/18/14 Pct Recovery = 105% Analysis Date = 09/13/14 Pct Recovery = 105% Analysis Date = 09/13/14 Pct Recovery = 105% Analysis Date = 09/08/14 Pct Recovery = 105% Analysis Date = 09/08/14 Pct Recovery = 105% Analysis Date = 09/04/14 Pct Recovery = 106% Analysis Date = 09/04/14 Pct Recovery = 106% Analysis Date = 08/30/14 Pct Recovery = 106% Analysis Date = 08/30/14 Pct Recovery = 106% Analysis Date = 08/25/14 Pct Recovery = 106% Analysis Date = 08/25/14 Pct Recovery = 106% Analysis Date = 08/20/14 Pct Recovery = 107% Analysis Date = 08/20/14 Pct Recovery = 107% Analysis Date = 08/15/14 Pct Recovery = 107% Analysis Date = 08/15/14 Pct Recovery = 107% Analysis Date = 08/11/14 Pct Recovery = 107% Analysis Date = 08/11/14 Pct Recovery = 107% Analysis Date = 08/06/14 Pct Recovery = 108% Analysis Date = 08/06/14 Pct Recovery = 108% Analysis Date = 08/01/14 Pct Recovery = 108% Analysis Date = 08/01/14 Pct Recovery = 108% Analysis Date = 07/27/14 Pct Recovery = 108% Analysis Date = 07/27/14 Pct Recovery = 108% Analysis Date = 07/23/14 Pct Recovery = 109% Analysis Date = 07/23/14 Pct Recovery = 109% Analysis Date = 07/18/14 Pct Recovery = 109% Analysis Date = 07/18/14 Pct Recovery = 109% Analysis Date = 07/13/14 Pct Recovery = 109% Analysis Date = 07/13/14 Pct Recovery = 109% Analysis Date = 07/08/14 Pct Recovery = 110% Analysis Date = 07/08/14 Pct Recovery = 110% Analysis Date = 07/04/14 Pct Recovery = 110% Analysis Date = 07/04/14 Pct Recovery = 110% Analysis Date = 06/29/14 Pct Recovery = 110% Analysis Date = 06/29/14 Pct Recovery = 110% Analysis Date = 06/24/14 Pct Recovery = 111% Analysis Date = 06/24/14 Pct Recovery = 111% Analysis Date = 06/19/14 Pct Recovery = 111% Analysis Date = 06/19/14 Pct Recovery = 111% Analysis Date = 06/14/14 Pct Recovery = 111% Analysis Date = 06/14/14 Pct Recovery = 111% Analysis Date = 06/10/14 Pct Recovery = 112% Analysis Date = 06/10/14 Pct Recovery = 112% Analysis Date = 06/05/14 Pct Recovery = 112% Analysis Date = 06/05/14 Pct Recovery = 112% Analysis Date = 05/31/14 Pct Recovery = 112% Analysis Date = 05/31/14 Pct Recovery = 112% Analysis Date = 05/26/14 Pct Recovery = 113% Analysis Date = 05/26/14 Pct Recovery = 113% Analysis Date = 05/22/14 Pct Recovery = 113% Analysis Date = 05/22/14 Pct Recovery = 113% Analysis Date = 05/17/14 Pct Recovery = 113% Analysis Date = 05/17/14 Pct Recovery = 113% Analysis Date = 05/12/14 Pct Recovery = 114% Analysis Date = 05/12/14 Pct Recovery = 114% Analysis Date = 05/07/14 Pct Recovery = 114% Analysis Date = 05/07/14 Pct Recovery = 114% Analysis Date = 05/03/14 Pct Recovery = 115% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
BROMOETHENE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 41 98% 16% 98% 10%
Total 41 98% 16% 98% 10%

Sample Statistics
BROMOETHENE

Characteristic N % % Basis
Plotted 41 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 41 .  
False Negatives 0 0% 0 out of 41
Not Spiked 32 .  
False Positives 0 0% 0 out of 32

BQS OBSP Determination:
BROMOFORM
METHOD: 4440 , TESTIDCODE: 32104GCM66
Open Data Set

Analysis Date = 12/16/16 SpikeMix = NSI 041816AVOC: 40 µl & ChemService 5082900: 40 µl Pct Recovery = 91% Analysis Date = 08/04/16 SpikeMix = Crescent 03FF058: 40 µl & Supelco LC20141V: 40 µl Pct Recovery = 87% Analysis Date = 07/20/16 SpikeMix = Supelco LC20141V: 40 µl & Accu 216041125: 40 µl Pct Recovery = 91% Analysis Date = 08/26/16 SpikeMix = NSI 041816AVOC: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 98% Analysis Date = 08/12/16 SpikeMix = ChemService 5082900: 25 µl & Phenova B20160319: 25 µl Pct Recovery = 90% Analysis Date = 06/30/16 SpikeMix = Crescent 03FF058: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 100% Analysis Date = 11/21/16 SpikeMix = Crescent 03FF058: 25 µl & Supelco LC20141V: 25 µl Pct Recovery = 84% Analysis Date = 09/08/16 SpikeMix = Supelco LC20141V: 25 µl & Accu 216041125: 25 µl Pct Recovery = 99% Analysis Date = 11/22/14 SpikeMix = NSI 032614: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 98% Analysis Date = 06/10/14 SpikeMix = Crescent 03DD004: 20 µl & NSI 032614: 20 µl Pct Recovery = 84% Analysis Date = 06/10/14 SpikeMix = NSI 032614: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 93% Analysis Date = 05/01/14 SpikeMix = Accu 214031115: 20 µl & NSI 032614: 20 µl Pct Recovery = 89% Analysis Date = 04/09/15 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 89% Analysis Date = 03/06/15 SpikeMix = ERA 0227-14-06.1A: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 99% Analysis Date = 11/14/14 SpikeMix = Crescent 03DD004: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 95% Analysis Date = 08/16/14 SpikeMix = ERA 0227-14-06.1A: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 97% Analysis Date = 07/01/14 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 107% Analysis Date = 09/29/15 SpikeMix = Accu 215041380: 25 µl & ERA 0406-15-03: 25 µl Pct Recovery = 82% Analysis Date = 06/16/15 SpikeMix = ERA 0406-15-03: 25 µl & Supelco LC13545: 25 µl Pct Recovery = 86% Analysis Date = 07/13/15 SpikeMix = Crescent 04EE008: 25 µl & NSI 050515AVOC: 25 µl Pct Recovery = 99% Analysis Date = 11/29/16 SpikeMix = ChemService 5082900: 15 µl & Phenova B20160319: 15 µl Pct Recovery = 83% Analysis Date = 09/28/16 SpikeMix = Crescent 03FF058: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 97% Analysis Date = 06/30/16 SpikeMix = ChemService 5082900: 15 µl & Accu 216041125: 15 µl Pct Recovery = 100% Analysis Date = 06/15/16 SpikeMix = NSI 041816AVOC: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 95% Analysis Date = 10/13/16 SpikeMix = NSI 041816AVOC: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 92% Analysis Date = 05/27/16 SpikeMix = Phenova B20160319: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 91% Analysis Date = 04/26/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 107% Analysis Date = 03/04/16 SpikeMix = Accu 215041380: 15 µl & ERA 0406-15-03: 15 µl Pct Recovery = 107% Analysis Date = 02/05/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 81% Analysis Date = 10/16/15 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 94% Analysis Date = 11/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 93% Analysis Date = 10/17/15 SpikeMix = Crescent 04EE008: 15 µl & NSI 050515AVOC: 15 µl Pct Recovery = 95% Analysis Date = 06/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Accu 215041380: 15 µl Pct Recovery = 91% Analysis Date = 09/09/14 SpikeMix = Accu 214031115: 10 µl & NSI 032614: 10 µl Pct Recovery = 97% Analysis Date = 09/09/14 SpikeMix = NSI 032614: 10 µl & Spex Organics C1140417015: 10 µl Pct Recovery = 102% Analysis Date = 07/29/14 SpikeMix = Crescent 03DD004: 10 µl & NSI 032614: 10 µl Pct Recovery = 107% Analysis Date = 05/30/14 SpikeMix = NSI 032614: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 101% Analysis Date = 01/13/15 SpikeMix = Accu 214031115: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 97% Analysis Date = 10/21/14 SpikeMix = ERA 0227-14-06.1A: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 94% Analysis Date = 10/04/14 SpikeMix = Crescent 03DD004: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 96% Analysis Date = 07/11/14 SpikeMix = Spex Organics C1140417015: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 96% Analysis Date = 11/20/15 SpikeMix = Accu 215041380: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 97% Analysis Date = 08/07/15 SpikeMix = Crescent 04EE008: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 79% Analysis Date = 06/27/15 SpikeMix = ERA 0406-15-03: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 94% Analysis Date = 03/17/16 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 123% Analysis Date = 01/27/16 SpikeMix = Crescent 04EE008: 10 µl & NSI 050515AVOC: 10 µl Pct Recovery = 101% Analysis Date = 12/10/15 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 107% Analysis Date = 09/03/15 SpikeMix = NSI 050515AVOC: 10 µl & Spex Organics EN150428007: 10 µl Pct Recovery = 109% Analysis Date = 12/15/16 Pct Recovery = 89% Analysis Date = 12/11/16 Pct Recovery = 89% Analysis Date = 12/11/16 Pct Recovery = 89% Analysis Date = 12/06/16 Pct Recovery = 89% Analysis Date = 12/06/16 Pct Recovery = 89% Analysis Date = 12/01/16 Pct Recovery = 90% Analysis Date = 12/01/16 Pct Recovery = 90% Analysis Date = 11/26/16 Pct Recovery = 90% Analysis Date = 11/26/16 Pct Recovery = 90% Analysis Date = 11/21/16 Pct Recovery = 90% Analysis Date = 11/21/16 Pct Recovery = 90% Analysis Date = 11/17/16 Pct Recovery = 90% Analysis Date = 11/17/16 Pct Recovery = 90% Analysis Date = 11/12/16 Pct Recovery = 90% Analysis Date = 11/12/16 Pct Recovery = 90% Analysis Date = 11/07/16 Pct Recovery = 91% Analysis Date = 11/07/16 Pct Recovery = 91% Analysis Date = 11/02/16 Pct Recovery = 91% Analysis Date = 11/02/16 Pct Recovery = 91% Analysis Date = 10/28/16 Pct Recovery = 91% Analysis Date = 10/28/16 Pct Recovery = 91% Analysis Date = 10/24/16 Pct Recovery = 91% Analysis Date = 10/24/16 Pct Recovery = 91% Analysis Date = 10/19/16 Pct Recovery = 92% Analysis Date = 10/19/16 Pct Recovery = 92% Analysis Date = 10/14/16 Pct Recovery = 92% Analysis Date = 10/14/16 Pct Recovery = 92% Analysis Date = 10/09/16 Pct Recovery = 92% Analysis Date = 10/09/16 Pct Recovery = 92% Analysis Date = 10/04/16 Pct Recovery = 92% Analysis Date = 10/04/16 Pct Recovery = 92% Analysis Date = 09/30/16 Pct Recovery = 92% Analysis Date = 09/30/16 Pct Recovery = 92% Analysis Date = 09/25/16 Pct Recovery = 92% Analysis Date = 09/25/16 Pct Recovery = 92% Analysis Date = 09/20/16 Pct Recovery = 93% Analysis Date = 09/20/16 Pct Recovery = 93% Analysis Date = 09/15/16 Pct Recovery = 93% Analysis Date = 09/15/16 Pct Recovery = 93% Analysis Date = 09/10/16 Pct Recovery = 93% Analysis Date = 09/10/16 Pct Recovery = 93% Analysis Date = 09/06/16 Pct Recovery = 93% Analysis Date = 09/06/16 Pct Recovery = 93% Analysis Date = 09/01/16 Pct Recovery = 93% Analysis Date = 09/01/16 Pct Recovery = 93% Analysis Date = 08/27/16 Pct Recovery = 94% Analysis Date = 08/27/16 Pct Recovery = 94% Analysis Date = 08/22/16 Pct Recovery = 94% Analysis Date = 08/22/16 Pct Recovery = 94% Analysis Date = 08/17/16 Pct Recovery = 94% Analysis Date = 08/17/16 Pct Recovery = 94% Analysis Date = 08/13/16 Pct Recovery = 94% Analysis Date = 08/13/16 Pct Recovery = 94% Analysis Date = 08/08/16 Pct Recovery = 94% Analysis Date = 08/08/16 Pct Recovery = 94% Analysis Date = 08/03/16 Pct Recovery = 94% Analysis Date = 08/03/16 Pct Recovery = 94% Analysis Date = 07/29/16 Pct Recovery = 95% Analysis Date = 07/29/16 Pct Recovery = 95% Analysis Date = 07/24/16 Pct Recovery = 95% Analysis Date = 07/24/16 Pct Recovery = 95% Analysis Date = 07/20/16 Pct Recovery = 95% Analysis Date = 07/20/16 Pct Recovery = 95% Analysis Date = 07/15/16 Pct Recovery = 95% Analysis Date = 07/15/16 Pct Recovery = 95% Analysis Date = 07/10/16 Pct Recovery = 95% Analysis Date = 07/10/16 Pct Recovery = 95% Analysis Date = 07/05/16 Pct Recovery = 95% Analysis Date = 07/05/16 Pct Recovery = 95% Analysis Date = 06/30/16 Pct Recovery = 96% Analysis Date = 06/30/16 Pct Recovery = 96% Analysis Date = 06/26/16 Pct Recovery = 96% Analysis Date = 06/26/16 Pct Recovery = 96% Analysis Date = 06/21/16 Pct Recovery = 96% Analysis Date = 06/21/16 Pct Recovery = 96% Analysis Date = 06/16/16 Pct Recovery = 96% Analysis Date = 06/16/16 Pct Recovery = 96% Analysis Date = 06/11/16 Pct Recovery = 96% Analysis Date = 06/11/16 Pct Recovery = 96% Analysis Date = 06/06/16 Pct Recovery = 96% Analysis Date = 06/06/16 Pct Recovery = 96% Analysis Date = 06/02/16 Pct Recovery = 96% Analysis Date = 06/02/16 Pct Recovery = 96% Analysis Date = 05/28/16 Pct Recovery = 96% Analysis Date = 05/28/16 Pct Recovery = 96% Analysis Date = 05/23/16 Pct Recovery = 97% Analysis Date = 05/23/16 Pct Recovery = 97% Analysis Date = 05/18/16 Pct Recovery = 97% Analysis Date = 05/18/16 Pct Recovery = 97% Analysis Date = 05/13/16 Pct Recovery = 97% Analysis Date = 05/13/16 Pct Recovery = 97% Analysis Date = 05/09/16 Pct Recovery = 97% Analysis Date = 05/09/16 Pct Recovery = 97% Analysis Date = 05/04/16 Pct Recovery = 97% Analysis Date = 05/04/16 Pct Recovery = 97% Analysis Date = 04/29/16 Pct Recovery = 97% Analysis Date = 04/29/16 Pct Recovery = 97% Analysis Date = 04/24/16 Pct Recovery = 97% Analysis Date = 04/24/16 Pct Recovery = 97% Analysis Date = 04/19/16 Pct Recovery = 97% Analysis Date = 04/19/16 Pct Recovery = 97% Analysis Date = 04/15/16 Pct Recovery = 97% Analysis Date = 04/15/16 Pct Recovery = 97% Analysis Date = 04/10/16 Pct Recovery = 98% Analysis Date = 04/10/16 Pct Recovery = 98% Analysis Date = 04/05/16 Pct Recovery = 98% Analysis Date = 04/05/16 Pct Recovery = 98% Analysis Date = 03/31/16 Pct Recovery = 98% Analysis Date = 03/31/16 Pct Recovery = 98% Analysis Date = 03/26/16 Pct Recovery = 98% Analysis Date = 03/26/16 Pct Recovery = 98% Analysis Date = 03/22/16 Pct Recovery = 98% Analysis Date = 03/22/16 Pct Recovery = 98% Analysis Date = 03/17/16 Pct Recovery = 98% Analysis Date = 03/17/16 Pct Recovery = 98% Analysis Date = 03/12/16 Pct Recovery = 98% Analysis Date = 03/12/16 Pct Recovery = 98% Analysis Date = 03/07/16 Pct Recovery = 98% Analysis Date = 03/07/16 Pct Recovery = 98% Analysis Date = 03/02/16 Pct Recovery = 98% Analysis Date = 03/02/16 Pct Recovery = 98% Analysis Date = 02/27/16 Pct Recovery = 98% Analysis Date = 02/27/16 Pct Recovery = 98% Analysis Date = 02/22/16 Pct Recovery = 98% Analysis Date = 02/22/16 Pct Recovery = 98% Analysis Date = 02/17/16 Pct Recovery = 98% Analysis Date = 02/17/16 Pct Recovery = 98% Analysis Date = 02/12/16 Pct Recovery = 98% Analysis Date = 02/12/16 Pct Recovery = 98% Analysis Date = 02/07/16 Pct Recovery = 98% Analysis Date = 02/07/16 Pct Recovery = 98% Analysis Date = 02/03/16 Pct Recovery = 98% Analysis Date = 02/03/16 Pct Recovery = 98% Analysis Date = 01/29/16 Pct Recovery = 98% Analysis Date = 01/29/16 Pct Recovery = 98% Analysis Date = 01/24/16 Pct Recovery = 98% Analysis Date = 01/24/16 Pct Recovery = 98% Analysis Date = 01/19/16 Pct Recovery = 98% Analysis Date = 01/19/16 Pct Recovery = 98% Analysis Date = 01/14/16 Pct Recovery = 98% Analysis Date = 01/14/16 Pct Recovery = 98% Analysis Date = 01/10/16 Pct Recovery = 98% Analysis Date = 01/10/16 Pct Recovery = 98% Analysis Date = 01/05/16 Pct Recovery = 98% Analysis Date = 01/05/16 Pct Recovery = 98% Analysis Date = 12/31/15 Pct Recovery = 97% Analysis Date = 12/31/15 Pct Recovery = 97% Analysis Date = 12/26/15 Pct Recovery = 97% Analysis Date = 12/26/15 Pct Recovery = 97% Analysis Date = 12/21/15 Pct Recovery = 97% Analysis Date = 12/21/15 Pct Recovery = 97% Analysis Date = 12/17/15 Pct Recovery = 97% Analysis Date = 12/17/15 Pct Recovery = 97% Analysis Date = 12/12/15 Pct Recovery = 97% Analysis Date = 12/12/15 Pct Recovery = 97% Analysis Date = 12/07/15 Pct Recovery = 97% Analysis Date = 12/07/15 Pct Recovery = 97% Analysis Date = 12/02/15 Pct Recovery = 97% Analysis Date = 12/02/15 Pct Recovery = 97% Analysis Date = 11/27/15 Pct Recovery = 97% Analysis Date = 11/27/15 Pct Recovery = 97% Analysis Date = 11/23/15 Pct Recovery = 97% Analysis Date = 11/23/15 Pct Recovery = 97% Analysis Date = 11/18/15 Pct Recovery = 97% Analysis Date = 11/18/15 Pct Recovery = 97% Analysis Date = 11/13/15 Pct Recovery = 96% Analysis Date = 11/13/15 Pct Recovery = 96% Analysis Date = 11/08/15 Pct Recovery = 96% Analysis Date = 11/08/15 Pct Recovery = 96% Analysis Date = 11/03/15 Pct Recovery = 96% Analysis Date = 11/03/15 Pct Recovery = 96% Analysis Date = 10/30/15 Pct Recovery = 96% Analysis Date = 10/30/15 Pct Recovery = 96% Analysis Date = 10/25/15 Pct Recovery = 96% Analysis Date = 10/25/15 Pct Recovery = 96% Analysis Date = 10/20/15 Pct Recovery = 96% Analysis Date = 10/20/15 Pct Recovery = 96% Analysis Date = 10/15/15 Pct Recovery = 96% Analysis Date = 10/15/15 Pct Recovery = 96% Analysis Date = 10/10/15 Pct Recovery = 96% Analysis Date = 10/10/15 Pct Recovery = 96% Analysis Date = 10/06/15 Pct Recovery = 95% Analysis Date = 10/06/15 Pct Recovery = 95% Analysis Date = 10/01/15 Pct Recovery = 95% Analysis Date = 10/01/15 Pct Recovery = 95% Analysis Date = 09/26/15 Pct Recovery = 95% Analysis Date = 09/26/15 Pct Recovery = 95% Analysis Date = 09/21/15 Pct Recovery = 95% Analysis Date = 09/21/15 Pct Recovery = 95% Analysis Date = 09/16/15 Pct Recovery = 95% Analysis Date = 09/16/15 Pct Recovery = 95% Analysis Date = 09/12/15 Pct Recovery = 95% Analysis Date = 09/12/15 Pct Recovery = 95% Analysis Date = 09/07/15 Pct Recovery = 95% Analysis Date = 09/07/15 Pct Recovery = 95% Analysis Date = 09/02/15 Pct Recovery = 95% Analysis Date = 09/02/15 Pct Recovery = 95% Analysis Date = 08/28/15 Pct Recovery = 95% Analysis Date = 08/28/15 Pct Recovery = 95% Analysis Date = 08/23/15 Pct Recovery = 95% Analysis Date = 08/23/15 Pct Recovery = 95% Analysis Date = 08/19/15 Pct Recovery = 95% Analysis Date = 08/19/15 Pct Recovery = 95% Analysis Date = 08/14/15 Pct Recovery = 95% Analysis Date = 08/14/15 Pct Recovery = 95% Analysis Date = 08/09/15 Pct Recovery = 94% Analysis Date = 08/09/15 Pct Recovery = 94% Analysis Date = 08/04/15 Pct Recovery = 94% Analysis Date = 08/04/15 Pct Recovery = 94% Analysis Date = 07/30/15 Pct Recovery = 94% Analysis Date = 07/30/15 Pct Recovery = 94% Analysis Date = 07/26/15 Pct Recovery = 94% Analysis Date = 07/26/15 Pct Recovery = 94% Analysis Date = 07/21/15 Pct Recovery = 94% Analysis Date = 07/21/15 Pct Recovery = 94% Analysis Date = 07/16/15 Pct Recovery = 94% Analysis Date = 07/16/15 Pct Recovery = 94% Analysis Date = 07/11/15 Pct Recovery = 94% Analysis Date = 07/11/15 Pct Recovery = 94% Analysis Date = 07/06/15 Pct Recovery = 94% Analysis Date = 07/06/15 Pct Recovery = 94% Analysis Date = 07/02/15 Pct Recovery = 94% Analysis Date = 07/02/15 Pct Recovery = 94% Analysis Date = 06/27/15 Pct Recovery = 94% Analysis Date = 06/27/15 Pct Recovery = 94% Analysis Date = 06/22/15 Pct Recovery = 94% Analysis Date = 06/22/15 Pct Recovery = 94% Analysis Date = 06/17/15 Pct Recovery = 94% Analysis Date = 06/17/15 Pct Recovery = 94% Analysis Date = 06/12/15 Pct Recovery = 94% Analysis Date = 06/12/15 Pct Recovery = 94% Analysis Date = 06/08/15 Pct Recovery = 94% Analysis Date = 06/08/15 Pct Recovery = 94% Analysis Date = 06/03/15 Pct Recovery = 94% Analysis Date = 06/03/15 Pct Recovery = 94% Analysis Date = 05/29/15 Pct Recovery = 94% Analysis Date = 05/29/15 Pct Recovery = 94% Analysis Date = 05/24/15 Pct Recovery = 94% Analysis Date = 05/24/15 Pct Recovery = 94% Analysis Date = 05/19/15 Pct Recovery = 94% Analysis Date = 05/19/15 Pct Recovery = 94% Analysis Date = 05/15/15 Pct Recovery = 94% Analysis Date = 05/15/15 Pct Recovery = 94% Analysis Date = 05/10/15 Pct Recovery = 94% Analysis Date = 05/10/15 Pct Recovery = 94% Analysis Date = 05/05/15 Pct Recovery = 94% Analysis Date = 05/05/15 Pct Recovery = 94% Analysis Date = 04/30/15 Pct Recovery = 94% Analysis Date = 04/30/15 Pct Recovery = 94% Analysis Date = 04/25/15 Pct Recovery = 94% Analysis Date = 04/25/15 Pct Recovery = 94% Analysis Date = 04/21/15 Pct Recovery = 94% Analysis Date = 04/21/15 Pct Recovery = 94% Analysis Date = 04/16/15 Pct Recovery = 94% Analysis Date = 04/16/15 Pct Recovery = 94% Analysis Date = 04/11/15 Pct Recovery = 94% Analysis Date = 04/11/15 Pct Recovery = 94% Analysis Date = 04/06/15 Pct Recovery = 94% Analysis Date = 04/06/15 Pct Recovery = 94% Analysis Date = 04/01/15 Pct Recovery = 95% Analysis Date = 04/01/15 Pct Recovery = 95% Analysis Date = 03/28/15 Pct Recovery = 95% Analysis Date = 03/28/15 Pct Recovery = 95% Analysis Date = 03/23/15 Pct Recovery = 95% Analysis Date = 03/23/15 Pct Recovery = 95% Analysis Date = 03/18/15 Pct Recovery = 95% Analysis Date = 03/18/15 Pct Recovery = 95% Analysis Date = 03/13/15 Pct Recovery = 95% Analysis Date = 03/13/15 Pct Recovery = 95% Analysis Date = 03/08/15 Pct Recovery = 95% Analysis Date = 03/08/15 Pct Recovery = 95% Analysis Date = 03/04/15 Pct Recovery = 95% Analysis Date = 03/04/15 Pct Recovery = 95% Analysis Date = 02/27/15 Pct Recovery = 95% Analysis Date = 02/27/15 Pct Recovery = 95% Analysis Date = 02/22/15 Pct Recovery = 95% Analysis Date = 02/22/15 Pct Recovery = 95% Analysis Date = 02/17/15 Pct Recovery = 95% Analysis Date = 02/17/15 Pct Recovery = 95% Analysis Date = 02/12/15 Pct Recovery = 95% Analysis Date = 02/12/15 Pct Recovery = 95% Analysis Date = 02/08/15 Pct Recovery = 95% Analysis Date = 02/08/15 Pct Recovery = 95% Analysis Date = 02/03/15 Pct Recovery = 95% Analysis Date = 02/03/15 Pct Recovery = 95% Analysis Date = 01/29/15 Pct Recovery = 95% Analysis Date = 01/29/15 Pct Recovery = 95% Analysis Date = 01/24/15 Pct Recovery = 95% Analysis Date = 01/24/15 Pct Recovery = 95% Analysis Date = 01/19/15 Pct Recovery = 95% Analysis Date = 01/19/15 Pct Recovery = 95% Analysis Date = 01/15/15 Pct Recovery = 95% Analysis Date = 01/15/15 Pct Recovery = 95% Analysis Date = 01/10/15 Pct Recovery = 95% Analysis Date = 01/10/15 Pct Recovery = 95% Analysis Date = 01/05/15 Pct Recovery = 95% Analysis Date = 01/05/15 Pct Recovery = 95% Analysis Date = 12/31/14 Pct Recovery = 95% Analysis Date = 12/31/14 Pct Recovery = 95% Analysis Date = 12/26/14 Pct Recovery = 95% Analysis Date = 12/26/14 Pct Recovery = 95% Analysis Date = 12/22/14 Pct Recovery = 95% Analysis Date = 12/22/14 Pct Recovery = 95% Analysis Date = 12/17/14 Pct Recovery = 95% Analysis Date = 12/17/14 Pct Recovery = 95% Analysis Date = 12/12/14 Pct Recovery = 96% Analysis Date = 12/12/14 Pct Recovery = 96% Analysis Date = 12/07/14 Pct Recovery = 96% Analysis Date = 12/07/14 Pct Recovery = 96% Analysis Date = 12/02/14 Pct Recovery = 96% Analysis Date = 12/02/14 Pct Recovery = 96% Analysis Date = 11/28/14 Pct Recovery = 96% Analysis Date = 11/28/14 Pct Recovery = 96% Analysis Date = 11/23/14 Pct Recovery = 96% Analysis Date = 11/23/14 Pct Recovery = 96% Analysis Date = 11/18/14 Pct Recovery = 96% Analysis Date = 11/18/14 Pct Recovery = 96% Analysis Date = 11/13/14 Pct Recovery = 96% Analysis Date = 11/13/14 Pct Recovery = 96% Analysis Date = 11/08/14 Pct Recovery = 96% Analysis Date = 11/08/14 Pct Recovery = 96% Analysis Date = 11/04/14 Pct Recovery = 96% Analysis Date = 11/04/14 Pct Recovery = 96% Analysis Date = 10/30/14 Pct Recovery = 96% Analysis Date = 10/30/14 Pct Recovery = 96% Analysis Date = 10/25/14 Pct Recovery = 96% Analysis Date = 10/25/14 Pct Recovery = 96% Analysis Date = 10/20/14 Pct Recovery = 96% Analysis Date = 10/20/14 Pct Recovery = 96% Analysis Date = 10/15/14 Pct Recovery = 96% Analysis Date = 10/15/14 Pct Recovery = 96% Analysis Date = 10/11/14 Pct Recovery = 96% Analysis Date = 10/11/14 Pct Recovery = 96% Analysis Date = 10/06/14 Pct Recovery = 96% Analysis Date = 10/06/14 Pct Recovery = 96% Analysis Date = 10/01/14 Pct Recovery = 96% Analysis Date = 10/01/14 Pct Recovery = 96% Analysis Date = 09/26/14 Pct Recovery = 96% Analysis Date = 09/26/14 Pct Recovery = 96% Analysis Date = 09/21/14 Pct Recovery = 96% Analysis Date = 09/21/14 Pct Recovery = 96% Analysis Date = 09/17/14 Pct Recovery = 96% Analysis Date = 09/17/14 Pct Recovery = 96% Analysis Date = 09/12/14 Pct Recovery = 96% Analysis Date = 09/12/14 Pct Recovery = 96% Analysis Date = 09/07/14 Pct Recovery = 96% Analysis Date = 09/07/14 Pct Recovery = 96% Analysis Date = 09/02/14 Pct Recovery = 96% Analysis Date = 09/02/14 Pct Recovery = 96% Analysis Date = 08/28/14 Pct Recovery = 96% Analysis Date = 08/28/14 Pct Recovery = 96% Analysis Date = 08/24/14 Pct Recovery = 96% Analysis Date = 08/24/14 Pct Recovery = 96% Analysis Date = 08/19/14 Pct Recovery = 97% Analysis Date = 08/19/14 Pct Recovery = 97% Analysis Date = 08/14/14 Pct Recovery = 97% Analysis Date = 08/14/14 Pct Recovery = 97% Analysis Date = 08/09/14 Pct Recovery = 97% Analysis Date = 08/09/14 Pct Recovery = 97% Analysis Date = 08/04/14 Pct Recovery = 97% Analysis Date = 08/04/14 Pct Recovery = 97% Analysis Date = 07/31/14 Pct Recovery = 97% Analysis Date = 07/31/14 Pct Recovery = 97% Analysis Date = 07/26/14 Pct Recovery = 97% Analysis Date = 07/26/14 Pct Recovery = 97% Analysis Date = 07/21/14 Pct Recovery = 97% Analysis Date = 07/21/14 Pct Recovery = 97% Analysis Date = 07/16/14 Pct Recovery = 97% Analysis Date = 07/16/14 Pct Recovery = 97% Analysis Date = 07/11/14 Pct Recovery = 97% Analysis Date = 07/11/14 Pct Recovery = 97% Analysis Date = 07/07/14 Pct Recovery = 97% Analysis Date = 07/07/14 Pct Recovery = 97% Analysis Date = 07/02/14 Pct Recovery = 97% Analysis Date = 07/02/14 Pct Recovery = 97% Analysis Date = 06/27/14 Pct Recovery = 97% Analysis Date = 06/27/14 Pct Recovery = 97% Analysis Date = 06/22/14 Pct Recovery = 97% Analysis Date = 06/22/14 Pct Recovery = 97% Analysis Date = 06/17/14 Pct Recovery = 97% Analysis Date = 06/17/14 Pct Recovery = 97% Analysis Date = 06/13/14 Pct Recovery = 97% Analysis Date = 06/13/14 Pct Recovery = 97% Analysis Date = 06/08/14 Pct Recovery = 97% Analysis Date = 06/08/14 Pct Recovery = 97% Analysis Date = 06/03/14 Pct Recovery = 97% Analysis Date = 06/03/14 Pct Recovery = 97% Analysis Date = 05/29/14 Pct Recovery = 97% Analysis Date = 05/29/14 Pct Recovery = 97% Analysis Date = 05/24/14 Pct Recovery = 97% Analysis Date = 05/24/14 Pct Recovery = 97% Analysis Date = 05/20/14 Pct Recovery = 97% Analysis Date = 05/20/14 Pct Recovery = 97% Analysis Date = 05/15/14 Pct Recovery = 97% Analysis Date = 05/15/14 Pct Recovery = 97% Analysis Date = 05/10/14 Pct Recovery = 97% Analysis Date = 05/10/14 Pct Recovery = 97% Analysis Date = 05/05/14 Pct Recovery = 97% Analysis Date = 05/05/14 Pct Recovery = 97% Analysis Date = 05/01/14 Pct Recovery = 97% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
BROMOFORM

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 48 95% 8% 96% 6%
Total 48 95% 8% 96% 6%

Sample Statistics
BROMOFORM

Characteristic N % % Basis
Plotted 48 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 48 .  
False Negatives 0 0% 0 out of 48
Not Spiked 25 .  
False Positives 0 0% 0 out of 25

BQS OBSP Determination:
BROMOMETHANE
METHOD: 4440 , TESTIDCODE: 34413GCM66
Open Data Set

Analysis Date = 12/12/16 SpikeMix = Accu 216041125: 40 µl & Crescent 03FF058: 40 µl Pct Recovery = 115% Analysis Date = 07/20/16 SpikeMix = Supelco LC20141V: 40 µl & Accu 216041125: 40 µl Pct Recovery = 127% Analysis Date = 07/14/16 SpikeMix = Accu 216041125: 40 µl & NSI 041816AVOC: 40 µl Pct Recovery = 75% Analysis Date = 09/08/16 SpikeMix = Supelco LC20141V: 25 µl & Accu 216041125: 25 µl Pct Recovery = 119% Analysis Date = 05/24/16 SpikeMix = Accu 216041125: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 119% Analysis Date = 08/12/16 SpikeMix = ChemService 5082900: 25 µl & Phenova B20160319: 25 µl Pct Recovery = 141% Analysis Date = 06/21/16 SpikeMix = Phenova B20160319: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 88% Analysis Date = 11/22/14 SpikeMix = NSI 032614: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 90% Analysis Date = 06/10/14 SpikeMix = Crescent 03DD004: 20 µl & NSI 032614: 20 µl Pct Recovery = 109% Analysis Date = 06/10/14 SpikeMix = NSI 032614: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 119% Analysis Date = 05/01/14 SpikeMix = Accu 214031115: 20 µl & NSI 032614: 20 µl Pct Recovery = 29% Analysis Date = 04/09/15 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 89% Analysis Date = 02/28/15 SpikeMix = ERA 0227-14-06.1A: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 124% Analysis Date = 11/14/14 SpikeMix = Crescent 03DD004: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 50% Analysis Date = 08/16/14 SpikeMix = ERA 0227-14-06.1A: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 129% Analysis Date = 07/01/14 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 49% Analysis Date = 09/29/15 SpikeMix = Accu 215041380: 25 µl & ERA 0406-15-03: 25 µl Pct Recovery = 99% Analysis Date = 08/15/15 SpikeMix = Supelco LC13545: 25 µl & Crescent 04EE008: 25 µl Pct Recovery = 113% Analysis Date = 07/18/15 SpikeMix = Crescent 04EE008: 25 µl & NSI 050515AVOC: 25 µl Pct Recovery = 68% Analysis Date = 10/13/16 SpikeMix = Accu 216041125: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 124% Analysis Date = 08/20/16 SpikeMix = Accu 216041125: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 106% Analysis Date = 07/06/16 SpikeMix = ChemService 5082900: 15 µl & Accu 216041125: 15 µl Pct Recovery = 160% Analysis Date = 11/29/16 SpikeMix = ChemService 5082900: 15 µl & Phenova B20160319: 15 µl Pct Recovery = 108% Analysis Date = 09/08/16 SpikeMix = Phenova B20160319: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 72% Analysis Date = 07/29/16 SpikeMix = Phenova B20160319: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 122% Analysis Date = 05/27/16 SpikeMix = Phenova B20160319: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 106% Analysis Date = 04/02/16 SpikeMix = Supelco LC13545: 15 µl & Accu 215041380: 15 µl Pct Recovery = 120% Analysis Date = 03/04/16 SpikeMix = Accu 215041380: 15 µl & ERA 0406-15-03: 15 µl Pct Recovery = 62% Analysis Date = 06/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Accu 215041380: 15 µl Pct Recovery = 105% Analysis Date = 12/18/15 SpikeMix = Supelco LC13545: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 110% Analysis Date = 10/17/15 SpikeMix = Crescent 04EE008: 15 µl & NSI 050515AVOC: 15 µl Pct Recovery = 56% Analysis Date = 06/29/15 SpikeMix = Spex Organics EN150428007: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 89% Analysis Date = 09/09/14 SpikeMix = Accu 214031115: 10 µl & NSI 032614: 10 µl Pct Recovery = 92% Analysis Date = 09/09/14 SpikeMix = NSI 032614: 10 µl & Spex Organics C1140417015: 10 µl Pct Recovery = 149% Analysis Date = 07/29/14 SpikeMix = Crescent 03DD004: 10 µl & NSI 032614: 10 µl Pct Recovery = 37% Analysis Date = 05/30/14 SpikeMix = NSI 032614: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 132% Analysis Date = 01/13/15 SpikeMix = Accu 214031115: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 65% Analysis Date = 10/21/14 SpikeMix = ERA 0227-14-06.1A: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 98% Analysis Date = 10/04/14 SpikeMix = Crescent 03DD004: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 58% Analysis Date = 07/11/14 SpikeMix = Spex Organics C1140417015: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 50% Analysis Date = 02/18/16 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 100% Analysis Date = 11/20/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 103% Analysis Date = 11/20/15 SpikeMix = Accu 215041380: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 83% Analysis Date = 06/04/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 97% Analysis Date = 05/13/16 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 87% Analysis Date = 01/27/16 SpikeMix = Crescent 04EE008: 10 µl & NSI 050515AVOC: 10 µl Pct Recovery = 84% Analysis Date = 07/31/15 SpikeMix = Crescent 04EE008: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 64% Analysis Date = 06/29/15 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 87% Analysis Date = 12/11/16 Pct Recovery = 119% Analysis Date = 12/07/16 Pct Recovery = 119% Analysis Date = 12/07/16 Pct Recovery = 119% Analysis Date = 12/02/16 Pct Recovery = 119% Analysis Date = 12/02/16 Pct Recovery = 119% Analysis Date = 11/27/16 Pct Recovery = 118% Analysis Date = 11/27/16 Pct Recovery = 118% Analysis Date = 11/22/16 Pct Recovery = 118% Analysis Date = 11/22/16 Pct Recovery = 118% Analysis Date = 11/18/16 Pct Recovery = 118% Analysis Date = 11/18/16 Pct Recovery = 118% Analysis Date = 11/13/16 Pct Recovery = 117% Analysis Date = 11/13/16 Pct Recovery = 117% Analysis Date = 11/08/16 Pct Recovery = 117% Analysis Date = 11/08/16 Pct Recovery = 117% Analysis Date = 11/03/16 Pct Recovery = 117% Analysis Date = 11/03/16 Pct Recovery = 117% Analysis Date = 10/29/16 Pct Recovery = 116% Analysis Date = 10/29/16 Pct Recovery = 116% Analysis Date = 10/25/16 Pct Recovery = 116% Analysis Date = 10/25/16 Pct Recovery = 116% Analysis Date = 10/20/16 Pct Recovery = 116% Analysis Date = 10/20/16 Pct Recovery = 116% Analysis Date = 10/15/16 Pct Recovery = 115% Analysis Date = 10/15/16 Pct Recovery = 115% Analysis Date = 10/10/16 Pct Recovery = 115% Analysis Date = 10/10/16 Pct Recovery = 115% Analysis Date = 10/06/16 Pct Recovery = 115% Analysis Date = 10/06/16 Pct Recovery = 115% Analysis Date = 10/01/16 Pct Recovery = 114% Analysis Date = 10/01/16 Pct Recovery = 114% Analysis Date = 09/26/16 Pct Recovery = 114% Analysis Date = 09/26/16 Pct Recovery = 114% Analysis Date = 09/21/16 Pct Recovery = 114% Analysis Date = 09/21/16 Pct Recovery = 114% Analysis Date = 09/16/16 Pct Recovery = 113% Analysis Date = 09/16/16 Pct Recovery = 113% Analysis Date = 09/12/16 Pct Recovery = 113% Analysis Date = 09/12/16 Pct Recovery = 113% Analysis Date = 09/07/16 Pct Recovery = 113% Analysis Date = 09/07/16 Pct Recovery = 113% Analysis Date = 09/02/16 Pct Recovery = 112% Analysis Date = 09/02/16 Pct Recovery = 112% Analysis Date = 08/28/16 Pct Recovery = 112% Analysis Date = 08/28/16 Pct Recovery = 112% Analysis Date = 08/24/16 Pct Recovery = 112% Analysis Date = 08/24/16 Pct Recovery = 112% Analysis Date = 08/19/16 Pct Recovery = 111% Analysis Date = 08/19/16 Pct Recovery = 111% Analysis Date = 08/14/16 Pct Recovery = 111% Analysis Date = 08/14/16 Pct Recovery = 111% Analysis Date = 08/09/16 Pct Recovery = 111% Analysis Date = 08/09/16 Pct Recovery = 111% Analysis Date = 08/04/16 Pct Recovery = 110% Analysis Date = 08/04/16 Pct Recovery = 110% Analysis Date = 07/31/16 Pct Recovery = 110% Analysis Date = 07/31/16 Pct Recovery = 110% Analysis Date = 07/26/16 Pct Recovery = 110% Analysis Date = 07/26/16 Pct Recovery = 110% Analysis Date = 07/21/16 Pct Recovery = 109% Analysis Date = 07/21/16 Pct Recovery = 109% Analysis Date = 07/16/16 Pct Recovery = 109% Analysis Date = 07/16/16 Pct Recovery = 109% Analysis Date = 07/12/16 Pct Recovery = 108% Analysis Date = 07/12/16 Pct Recovery = 108% Analysis Date = 07/07/16 Pct Recovery = 108% Analysis Date = 07/07/16 Pct Recovery = 108% Analysis Date = 07/02/16 Pct Recovery = 108% Analysis Date = 07/02/16 Pct Recovery = 108% Analysis Date = 06/27/16 Pct Recovery = 107% Analysis Date = 06/27/16 Pct Recovery = 107% Analysis Date = 06/22/16 Pct Recovery = 107% Analysis Date = 06/22/16 Pct Recovery = 107% Analysis Date = 06/18/16 Pct Recovery = 107% Analysis Date = 06/18/16 Pct Recovery = 107% Analysis Date = 06/13/16 Pct Recovery = 106% Analysis Date = 06/13/16 Pct Recovery = 106% Analysis Date = 06/08/16 Pct Recovery = 106% Analysis Date = 06/08/16 Pct Recovery = 106% Analysis Date = 06/03/16 Pct Recovery = 106% Analysis Date = 06/03/16 Pct Recovery = 106% Analysis Date = 05/30/16 Pct Recovery = 105% Analysis Date = 05/30/16 Pct Recovery = 105% Analysis Date = 05/25/16 Pct Recovery = 105% Analysis Date = 05/25/16 Pct Recovery = 105% Analysis Date = 05/20/16 Pct Recovery = 105% Analysis Date = 05/20/16 Pct Recovery = 105% Analysis Date = 05/15/16 Pct Recovery = 104% Analysis Date = 05/15/16 Pct Recovery = 104% Analysis Date = 05/10/16 Pct Recovery = 104% Analysis Date = 05/10/16 Pct Recovery = 104% Analysis Date = 05/06/16 Pct Recovery = 103% Analysis Date = 05/06/16 Pct Recovery = 103% Analysis Date = 05/01/16 Pct Recovery = 103% Analysis Date = 05/01/16 Pct Recovery = 103% Analysis Date = 04/26/16 Pct Recovery = 103% Analysis Date = 04/26/16 Pct Recovery = 103% Analysis Date = 04/21/16 Pct Recovery = 102% Analysis Date = 04/21/16 Pct Recovery = 102% Analysis Date = 04/16/16 Pct Recovery = 102% Analysis Date = 04/16/16 Pct Recovery = 102% Analysis Date = 04/12/16 Pct Recovery = 102% Analysis Date = 04/12/16 Pct Recovery = 102% Analysis Date = 04/07/16 Pct Recovery = 101% Analysis Date = 04/07/16 Pct Recovery = 101% Analysis Date = 04/02/16 Pct Recovery = 101% Analysis Date = 04/02/16 Pct Recovery = 101% Analysis Date = 03/28/16 Pct Recovery = 100% Analysis Date = 03/28/16 Pct Recovery = 100% Analysis Date = 03/24/16 Pct Recovery = 100% Analysis Date = 03/24/16 Pct Recovery = 100% Analysis Date = 03/19/16 Pct Recovery = 99% Analysis Date = 03/19/16 Pct Recovery = 99% Analysis Date = 03/14/16 Pct Recovery = 99% Analysis Date = 03/14/16 Pct Recovery = 99% Analysis Date = 03/09/16 Pct Recovery = 99% Analysis Date = 03/09/16 Pct Recovery = 99% Analysis Date = 03/04/16 Pct Recovery = 98% Analysis Date = 03/04/16 Pct Recovery = 98% Analysis Date = 02/29/16 Pct Recovery = 98% Analysis Date = 02/29/16 Pct Recovery = 98% Analysis Date = 02/24/16 Pct Recovery = 97% Analysis Date = 02/24/16 Pct Recovery = 97% Analysis Date = 02/19/16 Pct Recovery = 97% Analysis Date = 02/19/16 Pct Recovery = 97% Analysis Date = 02/14/16 Pct Recovery = 96% Analysis Date = 02/14/16 Pct Recovery = 96% Analysis Date = 02/10/16 Pct Recovery = 96% Analysis Date = 02/10/16 Pct Recovery = 96% Analysis Date = 02/05/16 Pct Recovery = 95% Analysis Date = 02/05/16 Pct Recovery = 95% Analysis Date = 01/31/16 Pct Recovery = 95% Analysis Date = 01/31/16 Pct Recovery = 95% Analysis Date = 01/26/16 Pct Recovery = 95% Analysis Date = 01/26/16 Pct Recovery = 95% Analysis Date = 01/21/16 Pct Recovery = 94% Analysis Date = 01/21/16 Pct Recovery = 94% Analysis Date = 01/17/16 Pct Recovery = 94% Analysis Date = 01/17/16 Pct Recovery = 94% Analysis Date = 01/12/16 Pct Recovery = 94% Analysis Date = 01/12/16 Pct Recovery = 94% Analysis Date = 01/07/16 Pct Recovery = 94% Analysis Date = 01/07/16 Pct Recovery = 94% Analysis Date = 01/02/16 Pct Recovery = 93% Analysis Date = 01/02/16 Pct Recovery = 93% Analysis Date = 12/29/15 Pct Recovery = 93% Analysis Date = 12/29/15 Pct Recovery = 93% Analysis Date = 12/24/15 Pct Recovery = 93% Analysis Date = 12/24/15 Pct Recovery = 93% Analysis Date = 12/19/15 Pct Recovery = 93% Analysis Date = 12/19/15 Pct Recovery = 93% Analysis Date = 12/14/15 Pct Recovery = 92% Analysis Date = 12/14/15 Pct Recovery = 92% Analysis Date = 12/09/15 Pct Recovery = 92% Analysis Date = 12/09/15 Pct Recovery = 92% Analysis Date = 12/05/15 Pct Recovery = 92% Analysis Date = 12/05/15 Pct Recovery = 92% Analysis Date = 11/30/15 Pct Recovery = 92% Analysis Date = 11/30/15 Pct Recovery = 92% Analysis Date = 11/25/15 Pct Recovery = 91% Analysis Date = 11/25/15 Pct Recovery = 91% Analysis Date = 11/20/15 Pct Recovery = 91% Analysis Date = 11/20/15 Pct Recovery = 91% Analysis Date = 11/16/15 Pct Recovery = 91% Analysis Date = 11/16/15 Pct Recovery = 91% Analysis Date = 11/11/15 Pct Recovery = 91% Analysis Date = 11/11/15 Pct Recovery = 91% Analysis Date = 11/06/15 Pct Recovery = 91% Analysis Date = 11/06/15 Pct Recovery = 91% Analysis Date = 11/01/15 Pct Recovery = 91% Analysis Date = 11/01/15 Pct Recovery = 91% Analysis Date = 10/27/15 Pct Recovery = 91% Analysis Date = 10/27/15 Pct Recovery = 91% Analysis Date = 10/23/15 Pct Recovery = 91% Analysis Date = 10/23/15 Pct Recovery = 91% Analysis Date = 10/18/15 Pct Recovery = 91% Analysis Date = 10/18/15 Pct Recovery = 91% Analysis Date = 10/13/15 Pct Recovery = 91% Analysis Date = 10/13/15 Pct Recovery = 91% Analysis Date = 10/08/15 Pct Recovery = 91% Analysis Date = 10/08/15 Pct Recovery = 91% Analysis Date = 10/04/15 Pct Recovery = 90% Analysis Date = 10/04/15 Pct Recovery = 90% Analysis Date = 09/29/15 Pct Recovery = 90% Analysis Date = 09/29/15 Pct Recovery = 90% Analysis Date = 09/24/15 Pct Recovery = 90% Analysis Date = 09/24/15 Pct Recovery = 90% Analysis Date = 09/19/15 Pct Recovery = 90% Analysis Date = 09/19/15 Pct Recovery = 90% Analysis Date = 09/14/15 Pct Recovery = 90% Analysis Date = 09/14/15 Pct Recovery = 90% Analysis Date = 09/10/15 Pct Recovery = 90% Analysis Date = 09/10/15 Pct Recovery = 90% Analysis Date = 09/05/15 Pct Recovery = 90% Analysis Date = 09/05/15 Pct Recovery = 90% Analysis Date = 08/31/15 Pct Recovery = 90% Analysis Date = 08/31/15 Pct Recovery = 90% Analysis Date = 08/26/15 Pct Recovery = 90% Analysis Date = 08/26/15 Pct Recovery = 90% Analysis Date = 08/21/15 Pct Recovery = 90% Analysis Date = 08/21/15 Pct Recovery = 90% Analysis Date = 08/17/15 Pct Recovery = 90% Analysis Date = 08/17/15 Pct Recovery = 90% Analysis Date = 08/12/15 Pct Recovery = 90% Analysis Date = 08/12/15 Pct Recovery = 90% Analysis Date = 08/07/15 Pct Recovery = 90% Analysis Date = 08/07/15 Pct Recovery = 90% Analysis Date = 08/02/15 Pct Recovery = 90% Analysis Date = 08/02/15 Pct Recovery = 90% Analysis Date = 07/29/15 Pct Recovery = 90% Analysis Date = 07/29/15 Pct Recovery = 90% Analysis Date = 07/24/15 Pct Recovery = 89% Analysis Date = 07/24/15 Pct Recovery = 89% Analysis Date = 07/19/15 Pct Recovery = 89% Analysis Date = 07/19/15 Pct Recovery = 89% Analysis Date = 07/14/15 Pct Recovery = 89% Analysis Date = 07/14/15 Pct Recovery = 89% Analysis Date = 07/09/15 Pct Recovery = 89% Analysis Date = 07/09/15 Pct Recovery = 89% Analysis Date = 07/05/15 Pct Recovery = 89% Analysis Date = 07/05/15 Pct Recovery = 89% Analysis Date = 06/30/15 Pct Recovery = 89% Analysis Date = 06/30/15 Pct Recovery = 89% Analysis Date = 06/25/15 Pct Recovery = 89% Analysis Date = 06/25/15 Pct Recovery = 89% Analysis Date = 06/20/15 Pct Recovery = 89% Analysis Date = 06/20/15 Pct Recovery = 89% Analysis Date = 06/16/15 Pct Recovery = 89% Analysis Date = 06/16/15 Pct Recovery = 89% Analysis Date = 06/11/15 Pct Recovery = 89% Analysis Date = 06/11/15 Pct Recovery = 89% Analysis Date = 06/06/15 Pct Recovery = 89% Analysis Date = 06/06/15 Pct Recovery = 89% Analysis Date = 06/01/15 Pct Recovery = 89% Analysis Date = 06/01/15 Pct Recovery = 89% Analysis Date = 05/27/15 Pct Recovery = 89% Analysis Date = 05/27/15 Pct Recovery = 89% Analysis Date = 05/23/15 Pct Recovery = 89% Analysis Date = 05/23/15 Pct Recovery = 89% Analysis Date = 05/18/15 Pct Recovery = 89% Analysis Date = 05/18/15 Pct Recovery = 89% Analysis Date = 05/13/15 Pct Recovery = 89% Analysis Date = 05/13/15 Pct Recovery = 89% Analysis Date = 05/08/15 Pct Recovery = 89% Analysis Date = 05/08/15 Pct Recovery = 89% Analysis Date = 05/04/15 Pct Recovery = 89% Analysis Date = 05/04/15 Pct Recovery = 89% Analysis Date = 04/29/15 Pct Recovery = 89% Analysis Date = 04/29/15 Pct Recovery = 89% Analysis Date = 04/24/15 Pct Recovery = 89% Analysis Date = 04/24/15 Pct Recovery = 89% Analysis Date = 04/19/15 Pct Recovery = 88% Analysis Date = 04/19/15 Pct Recovery = 88% Analysis Date = 04/14/15 Pct Recovery = 88% Analysis Date = 04/14/15 Pct Recovery = 88% Analysis Date = 04/10/15 Pct Recovery = 88% Analysis Date = 04/10/15 Pct Recovery = 88% Analysis Date = 04/05/15 Pct Recovery = 88% Analysis Date = 04/05/15 Pct Recovery = 88% Analysis Date = 03/31/15 Pct Recovery = 88% Analysis Date = 03/31/15 Pct Recovery = 88% Analysis Date = 03/26/15 Pct Recovery = 88% Analysis Date = 03/26/15 Pct Recovery = 88% Analysis Date = 03/22/15 Pct Recovery = 88% Analysis Date = 03/22/15 Pct Recovery = 88% Analysis Date = 03/17/15 Pct Recovery = 88% Analysis Date = 03/17/15 Pct Recovery = 88% Analysis Date = 03/12/15 Pct Recovery = 88% Analysis Date = 03/12/15 Pct Recovery = 88% Analysis Date = 03/07/15 Pct Recovery = 88% Analysis Date = 03/07/15 Pct Recovery = 88% Analysis Date = 03/02/15 Pct Recovery = 88% Analysis Date = 03/02/15 Pct Recovery = 88% Analysis Date = 02/26/15 Pct Recovery = 88% Analysis Date = 02/26/15 Pct Recovery = 88% Analysis Date = 02/21/15 Pct Recovery = 88% Analysis Date = 02/21/15 Pct Recovery = 88% Analysis Date = 02/16/15 Pct Recovery = 88% Analysis Date = 02/16/15 Pct Recovery = 88% Analysis Date = 02/11/15 Pct Recovery = 88% Analysis Date = 02/11/15 Pct Recovery = 88% Analysis Date = 02/07/15 Pct Recovery = 88% Analysis Date = 02/07/15 Pct Recovery = 88% Analysis Date = 02/02/15 Pct Recovery = 88% Analysis Date = 02/02/15 Pct Recovery = 88% Analysis Date = 01/28/15 Pct Recovery = 88% Analysis Date = 01/28/15 Pct Recovery = 88% Analysis Date = 01/23/15 Pct Recovery = 88% Analysis Date = 01/23/15 Pct Recovery = 88% Analysis Date = 01/18/15 Pct Recovery = 88% Analysis Date = 01/18/15 Pct Recovery = 88% Analysis Date = 01/14/15 Pct Recovery = 88% Analysis Date = 01/14/15 Pct Recovery = 88% Analysis Date = 01/09/15 Pct Recovery = 88% Analysis Date = 01/09/15 Pct Recovery = 88% Analysis Date = 01/04/15 Pct Recovery = 88% Analysis Date = 01/04/15 Pct Recovery = 88% Analysis Date = 12/30/14 Pct Recovery = 88% Analysis Date = 12/30/14 Pct Recovery = 88% Analysis Date = 12/25/14 Pct Recovery = 88% Analysis Date = 12/25/14 Pct Recovery = 88% Analysis Date = 12/21/14 Pct Recovery = 88% Analysis Date = 12/21/14 Pct Recovery = 88% Analysis Date = 12/16/14 Pct Recovery = 88% Analysis Date = 12/16/14 Pct Recovery = 88% Analysis Date = 12/11/14 Pct Recovery = 88% Analysis Date = 12/11/14 Pct Recovery = 88% Analysis Date = 12/06/14 Pct Recovery = 88% Analysis Date = 12/06/14 Pct Recovery = 88% Analysis Date = 12/02/14 Pct Recovery = 88% Analysis Date = 12/02/14 Pct Recovery = 88% Analysis Date = 11/27/14 Pct Recovery = 88% Analysis Date = 11/27/14 Pct Recovery = 88% Analysis Date = 11/22/14 Pct Recovery = 87% Analysis Date = 11/22/14 Pct Recovery = 87% Analysis Date = 11/17/14 Pct Recovery = 87% Analysis Date = 11/17/14 Pct Recovery = 87% Analysis Date = 11/12/14 Pct Recovery = 87% Analysis Date = 11/12/14 Pct Recovery = 87% Analysis Date = 11/08/14 Pct Recovery = 87% Analysis Date = 11/08/14 Pct Recovery = 87% Analysis Date = 11/03/14 Pct Recovery = 87% Analysis Date = 11/03/14 Pct Recovery = 87% Analysis Date = 10/29/14 Pct Recovery = 87% Analysis Date = 10/29/14 Pct Recovery = 87% Analysis Date = 10/24/14 Pct Recovery = 87% Analysis Date = 10/24/14 Pct Recovery = 87% Analysis Date = 10/20/14 Pct Recovery = 87% Analysis Date = 10/20/14 Pct Recovery = 87% Analysis Date = 10/15/14 Pct Recovery = 87% Analysis Date = 10/15/14 Pct Recovery = 87% Analysis Date = 10/10/14 Pct Recovery = 87% Analysis Date = 10/10/14 Pct Recovery = 87% Analysis Date = 10/05/14 Pct Recovery = 87% Analysis Date = 10/05/14 Pct Recovery = 87% Analysis Date = 09/30/14 Pct Recovery = 86% Analysis Date = 09/30/14 Pct Recovery = 86% Analysis Date = 09/26/14 Pct Recovery = 86% Analysis Date = 09/26/14 Pct Recovery = 86% Analysis Date = 09/21/14 Pct Recovery = 86% Analysis Date = 09/21/14 Pct Recovery = 86% Analysis Date = 09/16/14 Pct Recovery = 86% Analysis Date = 09/16/14 Pct Recovery = 86% Analysis Date = 09/11/14 Pct Recovery = 86% Analysis Date = 09/11/14 Pct Recovery = 86% Analysis Date = 09/07/14 Pct Recovery = 86% Analysis Date = 09/07/14 Pct Recovery = 86% Analysis Date = 09/02/14 Pct Recovery = 86% Analysis Date = 09/02/14 Pct Recovery = 86% Analysis Date = 08/28/14 Pct Recovery = 86% Analysis Date = 08/28/14 Pct Recovery = 86% Analysis Date = 08/23/14 Pct Recovery = 86% Analysis Date = 08/23/14 Pct Recovery = 86% Analysis Date = 08/18/14 Pct Recovery = 85% Analysis Date = 08/18/14 Pct Recovery = 85% Analysis Date = 08/14/14 Pct Recovery = 85% Analysis Date = 08/14/14 Pct Recovery = 85% Analysis Date = 08/09/14 Pct Recovery = 85% Analysis Date = 08/09/14 Pct Recovery = 85% Analysis Date = 08/04/14 Pct Recovery = 85% Analysis Date = 08/04/14 Pct Recovery = 85% Analysis Date = 07/30/14 Pct Recovery = 85% Analysis Date = 07/30/14 Pct Recovery = 85% Analysis Date = 07/26/14 Pct Recovery = 85% Analysis Date = 07/26/14 Pct Recovery = 85% Analysis Date = 07/21/14 Pct Recovery = 85% Analysis Date = 07/21/14 Pct Recovery = 85% Analysis Date = 07/16/14 Pct Recovery = 85% Analysis Date = 07/16/14 Pct Recovery = 85% Analysis Date = 07/11/14 Pct Recovery = 85% Analysis Date = 07/11/14 Pct Recovery = 85% Analysis Date = 07/06/14 Pct Recovery = 84% Analysis Date = 07/06/14 Pct Recovery = 84% Analysis Date = 07/02/14 Pct Recovery = 84% Analysis Date = 07/02/14 Pct Recovery = 84% Analysis Date = 06/27/14 Pct Recovery = 84% Analysis Date = 06/27/14 Pct Recovery = 84% Analysis Date = 06/22/14 Pct Recovery = 84% Analysis Date = 06/22/14 Pct Recovery = 84% Analysis Date = 06/17/14 Pct Recovery = 84% Analysis Date = 06/17/14 Pct Recovery = 84% Analysis Date = 06/13/14 Pct Recovery = 84% Analysis Date = 06/13/14 Pct Recovery = 84% Analysis Date = 06/08/14 Pct Recovery = 84% Analysis Date = 06/08/14 Pct Recovery = 84% Analysis Date = 06/03/14 Pct Recovery = 84% Analysis Date = 06/03/14 Pct Recovery = 84% Analysis Date = 05/29/14 Pct Recovery = 83% Analysis Date = 05/29/14 Pct Recovery = 83% Analysis Date = 05/24/14 Pct Recovery = 83% Analysis Date = 05/24/14 Pct Recovery = 83% Analysis Date = 05/20/14 Pct Recovery = 83% Analysis Date = 05/20/14 Pct Recovery = 83% Analysis Date = 05/15/14 Pct Recovery = 83% Analysis Date = 05/15/14 Pct Recovery = 83% Analysis Date = 05/10/14 Pct Recovery = 83% Analysis Date = 05/10/14 Pct Recovery = 83% Analysis Date = 05/05/14 Pct Recovery = 83% Analysis Date = 05/05/14 Pct Recovery = 83% Analysis Date = 05/01/14 Pct Recovery = 83% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
BROMOMETHANE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 48 95% 30% 98% 33%
Total 48 95% 30% 98% 33%

Sample Statistics
BROMOMETHANE

Characteristic N % % Basis
Plotted 48 100% Spiked
Estimated Values 48 100% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 48 .  
False Negatives 0 0% 0 out of 48
Not Spiked 25 .  
False Positives 17 68% 17 out of 25

BQS OBSP Determination:
BUTANE
METHOD: 4440 , TESTIDCODE: 81563GCM66
Open Data Set

Analysis Date = 08/15/15 SpikeMix = Supelco LC13545: 25 µl & Crescent 04EE008: 25 µl Pct Recovery = 103% Analysis Date = 07/13/15 SpikeMix = Crescent 04EE008: 25 µl & NSI 050515AVOC: 25 µl Pct Recovery = 88% Analysis Date = 09/29/15 SpikeMix = Accu 215041380: 25 µl & ERA 0406-15-03: 25 µl Pct Recovery = 56% Analysis Date = 12/18/15 SpikeMix = Supelco LC13545: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 97% Analysis Date = 10/17/15 SpikeMix = Crescent 04EE008: 15 µl & NSI 050515AVOC: 15 µl Pct Recovery = 77% Analysis Date = 05/09/15 SpikeMix = Spex Organics EN150428007: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 96% Analysis Date = 04/02/16 SpikeMix = Supelco LC13545: 15 µl & Accu 215041380: 15 µl Pct Recovery = 67% Analysis Date = 03/04/16 SpikeMix = Accu 215041380: 15 µl & ERA 0406-15-03: 15 µl Pct Recovery = 74% Analysis Date = 06/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Accu 215041380: 15 µl Pct Recovery = 68% Analysis Date = 01/27/16 SpikeMix = Crescent 04EE008: 10 µl & NSI 050515AVOC: 10 µl Pct Recovery = 96% Analysis Date = 07/31/15 SpikeMix = Crescent 04EE008: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 104% Analysis Date = 05/09/15 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 95% Analysis Date = 02/18/16 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 63% Analysis Date = 11/20/15 SpikeMix = Accu 215041380: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 80% Analysis Date = 11/12/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 81% Analysis Date = 05/21/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 58% Analysis Date = 04/02/16 Pct Recovery = 67% Analysis Date = 03/31/16 Pct Recovery = 68% Analysis Date = 03/31/16 Pct Recovery = 68% Analysis Date = 03/29/16 Pct Recovery = 68% Analysis Date = 03/29/16 Pct Recovery = 68% Analysis Date = 03/28/16 Pct Recovery = 68% Analysis Date = 03/28/16 Pct Recovery = 68% Analysis Date = 03/26/16 Pct Recovery = 69% Analysis Date = 03/26/16 Pct Recovery = 69% Analysis Date = 03/24/16 Pct Recovery = 69% Analysis Date = 03/24/16 Pct Recovery = 69% Analysis Date = 03/23/16 Pct Recovery = 70% Analysis Date = 03/23/16 Pct Recovery = 70% Analysis Date = 03/21/16 Pct Recovery = 70% Analysis Date = 03/21/16 Pct Recovery = 70% Analysis Date = 03/19/16 Pct Recovery = 70% Analysis Date = 03/19/16 Pct Recovery = 70% Analysis Date = 03/18/16 Pct Recovery = 71% Analysis Date = 03/18/16 Pct Recovery = 71% Analysis Date = 03/16/16 Pct Recovery = 71% Analysis Date = 03/16/16 Pct Recovery = 71% Analysis Date = 03/14/16 Pct Recovery = 71% Analysis Date = 03/14/16 Pct Recovery = 71% Analysis Date = 03/13/16 Pct Recovery = 72% Analysis Date = 03/13/16 Pct Recovery = 72% Analysis Date = 03/11/16 Pct Recovery = 72% Analysis Date = 03/11/16 Pct Recovery = 72% Analysis Date = 03/09/16 Pct Recovery = 72% Analysis Date = 03/09/16 Pct Recovery = 72% Analysis Date = 03/08/16 Pct Recovery = 73% Analysis Date = 03/08/16 Pct Recovery = 73% Analysis Date = 03/06/16 Pct Recovery = 73% Analysis Date = 03/06/16 Pct Recovery = 73% Analysis Date = 03/05/16 Pct Recovery = 73% Analysis Date = 03/05/16 Pct Recovery = 73% Analysis Date = 03/03/16 Pct Recovery = 74% Analysis Date = 03/03/16 Pct Recovery = 74% Analysis Date = 03/01/16 Pct Recovery = 74% Analysis Date = 03/01/16 Pct Recovery = 74% Analysis Date = 02/29/16 Pct Recovery = 74% Analysis Date = 02/29/16 Pct Recovery = 74% Analysis Date = 02/27/16 Pct Recovery = 74% Analysis Date = 02/27/16 Pct Recovery = 74% Analysis Date = 02/25/16 Pct Recovery = 75% Analysis Date = 02/25/16 Pct Recovery = 75% Analysis Date = 02/24/16 Pct Recovery = 75% Analysis Date = 02/24/16 Pct Recovery = 75% Analysis Date = 02/22/16 Pct Recovery = 75% Analysis Date = 02/22/16 Pct Recovery = 75% Analysis Date = 02/20/16 Pct Recovery = 76% Analysis Date = 02/20/16 Pct Recovery = 76% Analysis Date = 02/19/16 Pct Recovery = 76% Analysis Date = 02/19/16 Pct Recovery = 76% Analysis Date = 02/17/16 Pct Recovery = 76% Analysis Date = 02/17/16 Pct Recovery = 76% Analysis Date = 02/15/16 Pct Recovery = 77% Analysis Date = 02/15/16 Pct Recovery = 77% Analysis Date = 02/14/16 Pct Recovery = 77% Analysis Date = 02/14/16 Pct Recovery = 77% Analysis Date = 02/12/16 Pct Recovery = 77% Analysis Date = 02/12/16 Pct Recovery = 77% Analysis Date = 02/11/16 Pct Recovery = 77% Analysis Date = 02/11/16 Pct Recovery = 77% Analysis Date = 02/09/16 Pct Recovery = 78% Analysis Date = 02/09/16 Pct Recovery = 78% Analysis Date = 02/07/16 Pct Recovery = 78% Analysis Date = 02/07/16 Pct Recovery = 78% Analysis Date = 02/06/16 Pct Recovery = 78% Analysis Date = 02/06/16 Pct Recovery = 78% Analysis Date = 02/04/16 Pct Recovery = 79% Analysis Date = 02/04/16 Pct Recovery = 79% Analysis Date = 02/02/16 Pct Recovery = 79% Analysis Date = 02/02/16 Pct Recovery = 79% Analysis Date = 02/01/16 Pct Recovery = 79% Analysis Date = 02/01/16 Pct Recovery = 79% Analysis Date = 01/30/16 Pct Recovery = 79% Analysis Date = 01/30/16 Pct Recovery = 79% Analysis Date = 01/28/16 Pct Recovery = 80% Analysis Date = 01/28/16 Pct Recovery = 80% Analysis Date = 01/27/16 Pct Recovery = 80% Analysis Date = 01/27/16 Pct Recovery = 80% Analysis Date = 01/25/16 Pct Recovery = 80% Analysis Date = 01/25/16 Pct Recovery = 80% Analysis Date = 01/23/16 Pct Recovery = 80% Analysis Date = 01/23/16 Pct Recovery = 80% Analysis Date = 01/22/16 Pct Recovery = 80% Analysis Date = 01/22/16 Pct Recovery = 80% Analysis Date = 01/20/16 Pct Recovery = 80% Analysis Date = 01/20/16 Pct Recovery = 80% Analysis Date = 01/18/16 Pct Recovery = 81% Analysis Date = 01/18/16 Pct Recovery = 81% Analysis Date = 01/17/16 Pct Recovery = 81% Analysis Date = 01/17/16 Pct Recovery = 81% Analysis Date = 01/15/16 Pct Recovery = 81% Analysis Date = 01/15/16 Pct Recovery = 81% Analysis Date = 01/14/16 Pct Recovery = 81% Analysis Date = 01/14/16 Pct Recovery = 81% Analysis Date = 01/12/16 Pct Recovery = 81% Analysis Date = 01/12/16 Pct Recovery = 81% Analysis Date = 01/10/16 Pct Recovery = 81% Analysis Date = 01/10/16 Pct Recovery = 81% Analysis Date = 01/09/16 Pct Recovery = 81% Analysis Date = 01/09/16 Pct Recovery = 81% Analysis Date = 01/07/16 Pct Recovery = 81% Analysis Date = 01/07/16 Pct Recovery = 81% Analysis Date = 01/05/16 Pct Recovery = 82% Analysis Date = 01/05/16 Pct Recovery = 82% Analysis Date = 01/04/16 Pct Recovery = 82% Analysis Date = 01/04/16 Pct Recovery = 82% Analysis Date = 01/02/16 Pct Recovery = 82% Analysis Date = 01/02/16 Pct Recovery = 82% Analysis Date = 12/31/15 Pct Recovery = 82% Analysis Date = 12/31/15 Pct Recovery = 82% Analysis Date = 12/30/15 Pct Recovery = 82% Analysis Date = 12/30/15 Pct Recovery = 82% Analysis Date = 12/28/15 Pct Recovery = 82% Analysis Date = 12/28/15 Pct Recovery = 82% Analysis Date = 12/26/15 Pct Recovery = 82% Analysis Date = 12/26/15 Pct Recovery = 82% Analysis Date = 12/25/15 Pct Recovery = 83% Analysis Date = 12/25/15 Pct Recovery = 83% Analysis Date = 12/23/15 Pct Recovery = 83% Analysis Date = 12/23/15 Pct Recovery = 83% Analysis Date = 12/22/15 Pct Recovery = 83% Analysis Date = 12/22/15 Pct Recovery = 83% Analysis Date = 12/20/15 Pct Recovery = 83% Analysis Date = 12/20/15 Pct Recovery = 83% Analysis Date = 12/18/15 Pct Recovery = 83% Analysis Date = 12/18/15 Pct Recovery = 83% Analysis Date = 12/17/15 Pct Recovery = 83% Analysis Date = 12/17/15 Pct Recovery = 83% Analysis Date = 12/15/15 Pct Recovery = 83% Analysis Date = 12/15/15 Pct Recovery = 83% Analysis Date = 12/13/15 Pct Recovery = 83% Analysis Date = 12/13/15 Pct Recovery = 83% Analysis Date = 12/12/15 Pct Recovery = 83% Analysis Date = 12/12/15 Pct Recovery = 83% Analysis Date = 12/10/15 Pct Recovery = 83% Analysis Date = 12/10/15 Pct Recovery = 83% Analysis Date = 12/08/15 Pct Recovery = 83% Analysis Date = 12/08/15 Pct Recovery = 83% Analysis Date = 12/07/15 Pct Recovery = 83% Analysis Date = 12/07/15 Pct Recovery = 83% Analysis Date = 12/05/15 Pct Recovery = 83% Analysis Date = 12/05/15 Pct Recovery = 83% Analysis Date = 12/03/15 Pct Recovery = 82% Analysis Date = 12/03/15 Pct Recovery = 82% Analysis Date = 12/02/15 Pct Recovery = 82% Analysis Date = 12/02/15 Pct Recovery = 82% Analysis Date = 11/30/15 Pct Recovery = 82% Analysis Date = 11/30/15 Pct Recovery = 82% Analysis Date = 11/28/15 Pct Recovery = 82% Analysis Date = 11/28/15 Pct Recovery = 82% Analysis Date = 11/27/15 Pct Recovery = 82% Analysis Date = 11/27/15 Pct Recovery = 82% Analysis Date = 11/25/15 Pct Recovery = 82% Analysis Date = 11/25/15 Pct Recovery = 82% Analysis Date = 11/24/15 Pct Recovery = 82% Analysis Date = 11/24/15 Pct Recovery = 82% Analysis Date = 11/22/15 Pct Recovery = 82% Analysis Date = 11/22/15 Pct Recovery = 82% Analysis Date = 11/20/15 Pct Recovery = 82% Analysis Date = 11/20/15 Pct Recovery = 82% Analysis Date = 11/19/15 Pct Recovery = 82% Analysis Date = 11/19/15 Pct Recovery = 82% Analysis Date = 11/17/15 Pct Recovery = 81% Analysis Date = 11/17/15 Pct Recovery = 81% Analysis Date = 11/15/15 Pct Recovery = 81% Analysis Date = 11/15/15 Pct Recovery = 81% Analysis Date = 11/14/15 Pct Recovery = 81% Analysis Date = 11/14/15 Pct Recovery = 81% Analysis Date = 11/12/15 Pct Recovery = 80% Analysis Date = 11/12/15 Pct Recovery = 80% Analysis Date = 11/10/15 Pct Recovery = 80% Analysis Date = 11/10/15 Pct Recovery = 80% Analysis Date = 11/09/15 Pct Recovery = 80% Analysis Date = 11/09/15 Pct Recovery = 80% Analysis Date = 11/07/15 Pct Recovery = 80% Analysis Date = 11/07/15 Pct Recovery = 80% Analysis Date = 11/05/15 Pct Recovery = 80% Analysis Date = 11/05/15 Pct Recovery = 80% Analysis Date = 11/04/15 Pct Recovery = 80% Analysis Date = 11/04/15 Pct Recovery = 80% Analysis Date = 11/02/15 Pct Recovery = 80% Analysis Date = 11/02/15 Pct Recovery = 80% Analysis Date = 11/01/15 Pct Recovery = 80% Analysis Date = 11/01/15 Pct Recovery = 80% Analysis Date = 10/30/15 Pct Recovery = 80% Analysis Date = 10/30/15 Pct Recovery = 80% Analysis Date = 10/28/15 Pct Recovery = 80% Analysis Date = 10/28/15 Pct Recovery = 80% Analysis Date = 10/27/15 Pct Recovery = 80% Analysis Date = 10/27/15 Pct Recovery = 80% Analysis Date = 10/25/15 Pct Recovery = 80% Analysis Date = 10/25/15 Pct Recovery = 80% Analysis Date = 10/23/15 Pct Recovery = 79% Analysis Date = 10/23/15 Pct Recovery = 79% Analysis Date = 10/22/15 Pct Recovery = 79% Analysis Date = 10/22/15 Pct Recovery = 79% Analysis Date = 10/20/15 Pct Recovery = 79% Analysis Date = 10/20/15 Pct Recovery = 79% Analysis Date = 10/18/15 Pct Recovery = 79% Analysis Date = 10/18/15 Pct Recovery = 79% Analysis Date = 10/17/15 Pct Recovery = 79% Analysis Date = 10/17/15 Pct Recovery = 79% Analysis Date = 10/15/15 Pct Recovery = 80% Analysis Date = 10/15/15 Pct Recovery = 80% Analysis Date = 10/13/15 Pct Recovery = 80% Analysis Date = 10/13/15 Pct Recovery = 80% Analysis Date = 10/12/15 Pct Recovery = 80% Analysis Date = 10/12/15 Pct Recovery = 80% Analysis Date = 10/10/15 Pct Recovery = 81% Analysis Date = 10/10/15 Pct Recovery = 81% Analysis Date = 10/08/15 Pct Recovery = 81% Analysis Date = 10/08/15 Pct Recovery = 81% Analysis Date = 10/07/15 Pct Recovery = 81% Analysis Date = 10/07/15 Pct Recovery = 81% Analysis Date = 10/05/15 Pct Recovery = 82% Analysis Date = 10/05/15 Pct Recovery = 82% Analysis Date = 10/04/15 Pct Recovery = 82% Analysis Date = 10/04/15 Pct Recovery = 82% Analysis Date = 10/02/15 Pct Recovery = 83% Analysis Date = 10/02/15 Pct Recovery = 83% Analysis Date = 09/30/15 Pct Recovery = 83% Analysis Date = 09/30/15 Pct Recovery = 83% Analysis Date = 09/29/15 Pct Recovery = 83% Analysis Date = 09/29/15 Pct Recovery = 83% Analysis Date = 09/27/15 Pct Recovery = 83% Analysis Date = 09/27/15 Pct Recovery = 83% Analysis Date = 09/25/15 Pct Recovery = 84% Analysis Date = 09/25/15 Pct Recovery = 84% Analysis Date = 09/24/15 Pct Recovery = 84% Analysis Date = 09/24/15 Pct Recovery = 84% Analysis Date = 09/22/15 Pct Recovery = 84% Analysis Date = 09/22/15 Pct Recovery = 84% Analysis Date = 09/20/15 Pct Recovery = 84% Analysis Date = 09/20/15 Pct Recovery = 84% Analysis Date = 09/19/15 Pct Recovery = 84% Analysis Date = 09/19/15 Pct Recovery = 84% Analysis Date = 09/17/15 Pct Recovery = 84% Analysis Date = 09/17/15 Pct Recovery = 84% Analysis Date = 09/15/15 Pct Recovery = 85% Analysis Date = 09/15/15 Pct Recovery = 85% Analysis Date = 09/14/15 Pct Recovery = 85% Analysis Date = 09/14/15 Pct Recovery = 85% Analysis Date = 09/12/15 Pct Recovery = 85% Analysis Date = 09/12/15 Pct Recovery = 85% Analysis Date = 09/11/15 Pct Recovery = 85% Analysis Date = 09/11/15 Pct Recovery = 85% Analysis Date = 09/09/15 Pct Recovery = 85% Analysis Date = 09/09/15 Pct Recovery = 85% Analysis Date = 09/07/15 Pct Recovery = 85% Analysis Date = 09/07/15 Pct Recovery = 85% Analysis Date = 09/06/15 Pct Recovery = 85% Analysis Date = 09/06/15 Pct Recovery = 85% Analysis Date = 09/04/15 Pct Recovery = 86% Analysis Date = 09/04/15 Pct Recovery = 86% Analysis Date = 09/02/15 Pct Recovery = 86% Analysis Date = 09/02/15 Pct Recovery = 86% Analysis Date = 09/01/15 Pct Recovery = 86% Analysis Date = 09/01/15 Pct Recovery = 86% Analysis Date = 08/30/15 Pct Recovery = 86% Analysis Date = 08/30/15 Pct Recovery = 86% Analysis Date = 08/28/15 Pct Recovery = 86% Analysis Date = 08/28/15 Pct Recovery = 86% Analysis Date = 08/27/15 Pct Recovery = 86% Analysis Date = 08/27/15 Pct Recovery = 86% Analysis Date = 08/25/15 Pct Recovery = 86% Analysis Date = 08/25/15 Pct Recovery = 86% Analysis Date = 08/23/15 Pct Recovery = 87% Analysis Date = 08/23/15 Pct Recovery = 87% Analysis Date = 08/22/15 Pct Recovery = 87% Analysis Date = 08/22/15 Pct Recovery = 87% Analysis Date = 08/20/15 Pct Recovery = 87% Analysis Date = 08/20/15 Pct Recovery = 87% Analysis Date = 08/18/15 Pct Recovery = 87% Analysis Date = 08/18/15 Pct Recovery = 87% Analysis Date = 08/17/15 Pct Recovery = 87% Analysis Date = 08/17/15 Pct Recovery = 87% Analysis Date = 08/15/15 Pct Recovery = 87% Analysis Date = 08/15/15 Pct Recovery = 87% Analysis Date = 08/14/15 Pct Recovery = 88% Analysis Date = 08/14/15 Pct Recovery = 88% Analysis Date = 08/12/15 Pct Recovery = 88% Analysis Date = 08/12/15 Pct Recovery = 88% Analysis Date = 08/10/15 Pct Recovery = 89% Analysis Date = 08/10/15 Pct Recovery = 89% Analysis Date = 08/09/15 Pct Recovery = 89% Analysis Date = 08/09/15 Pct Recovery = 89% Analysis Date = 08/07/15 Pct Recovery = 90% Analysis Date = 08/07/15 Pct Recovery = 90% Analysis Date = 08/05/15 Pct Recovery = 91% Analysis Date = 08/05/15 Pct Recovery = 91% Analysis Date = 08/04/15 Pct Recovery = 91% Analysis Date = 08/04/15 Pct Recovery = 91% Analysis Date = 08/02/15 Pct Recovery = 92% Analysis Date = 08/02/15 Pct Recovery = 92% Analysis Date = 07/31/15 Pct Recovery = 92% Analysis Date = 07/31/15 Pct Recovery = 92% Analysis Date = 07/30/15 Pct Recovery = 93% Analysis Date = 07/30/15 Pct Recovery = 93% Analysis Date = 07/28/15 Pct Recovery = 92% Analysis Date = 07/28/15 Pct Recovery = 92% Analysis Date = 07/26/15 Pct Recovery = 92% Analysis Date = 07/26/15 Pct Recovery = 92% Analysis Date = 07/25/15 Pct Recovery = 92% Analysis Date = 07/25/15 Pct Recovery = 92% Analysis Date = 07/23/15 Pct Recovery = 91% Analysis Date = 07/23/15 Pct Recovery = 91% Analysis Date = 07/22/15 Pct Recovery = 91% Analysis Date = 07/22/15 Pct Recovery = 91% Analysis Date = 07/20/15 Pct Recovery = 91% Analysis Date = 07/20/15 Pct Recovery = 91% Analysis Date = 07/18/15 Pct Recovery = 91% Analysis Date = 07/18/15 Pct Recovery = 91% Analysis Date = 07/17/15 Pct Recovery = 90% Analysis Date = 07/17/15 Pct Recovery = 90% Analysis Date = 07/15/15 Pct Recovery = 90% Analysis Date = 07/15/15 Pct Recovery = 90% Analysis Date = 07/13/15 Pct Recovery = 90% Analysis Date = 07/13/15 Pct Recovery = 90% Analysis Date = 07/12/15 Pct Recovery = 90% Analysis Date = 07/12/15 Pct Recovery = 90% Analysis Date = 07/10/15 Pct Recovery = 89% Analysis Date = 07/10/15 Pct Recovery = 89% Analysis Date = 07/08/15 Pct Recovery = 89% Analysis Date = 07/08/15 Pct Recovery = 89% Analysis Date = 07/07/15 Pct Recovery = 89% Analysis Date = 07/07/15 Pct Recovery = 89% Analysis Date = 07/05/15 Pct Recovery = 89% Analysis Date = 07/05/15 Pct Recovery = 89% Analysis Date = 07/03/15 Pct Recovery = 88% Analysis Date = 07/03/15 Pct Recovery = 88% Analysis Date = 07/02/15 Pct Recovery = 88% Analysis Date = 07/02/15 Pct Recovery = 88% Analysis Date = 06/30/15 Pct Recovery = 88% Analysis Date = 06/30/15 Pct Recovery = 88% Analysis Date = 06/28/15 Pct Recovery = 88% Analysis Date = 06/28/15 Pct Recovery = 88% Analysis Date = 06/27/15 Pct Recovery = 87% Analysis Date = 06/27/15 Pct Recovery = 87% Analysis Date = 06/25/15 Pct Recovery = 87% Analysis Date = 06/25/15 Pct Recovery = 87% Analysis Date = 06/24/15 Pct Recovery = 87% Analysis Date = 06/24/15 Pct Recovery = 87% Analysis Date = 06/22/15 Pct Recovery = 87% Analysis Date = 06/22/15 Pct Recovery = 87% Analysis Date = 06/20/15 Pct Recovery = 86% Analysis Date = 06/20/15 Pct Recovery = 86% Analysis Date = 06/19/15 Pct Recovery = 86% Analysis Date = 06/19/15 Pct Recovery = 86% Analysis Date = 06/17/15 Pct Recovery = 86% Analysis Date = 06/17/15 Pct Recovery = 86% Analysis Date = 06/15/15 Pct Recovery = 86% Analysis Date = 06/15/15 Pct Recovery = 86% Analysis Date = 06/14/15 Pct Recovery = 85% Analysis Date = 06/14/15 Pct Recovery = 85% Analysis Date = 06/12/15 Pct Recovery = 85% Analysis Date = 06/12/15 Pct Recovery = 85% Analysis Date = 06/10/15 Pct Recovery = 85% Analysis Date = 06/10/15 Pct Recovery = 85% Analysis Date = 06/09/15 Pct Recovery = 85% Analysis Date = 06/09/15 Pct Recovery = 85% Analysis Date = 06/07/15 Pct Recovery = 84% Analysis Date = 06/07/15 Pct Recovery = 84% Analysis Date = 06/05/15 Pct Recovery = 84% Analysis Date = 06/05/15 Pct Recovery = 84% Analysis Date = 06/04/15 Pct Recovery = 84% Analysis Date = 06/04/15 Pct Recovery = 84% Analysis Date = 06/02/15 Pct Recovery = 84% Analysis Date = 06/02/15 Pct Recovery = 84% Analysis Date = 06/01/15 Pct Recovery = 83% Analysis Date = 06/01/15 Pct Recovery = 83% Analysis Date = 05/30/15 Pct Recovery = 83% Analysis Date = 05/30/15 Pct Recovery = 83% Analysis Date = 05/28/15 Pct Recovery = 83% Analysis Date = 05/28/15 Pct Recovery = 83% Analysis Date = 05/27/15 Pct Recovery = 83% Analysis Date = 05/27/15 Pct Recovery = 83% Analysis Date = 05/25/15 Pct Recovery = 82% Analysis Date = 05/25/15 Pct Recovery = 82% Analysis Date = 05/23/15 Pct Recovery = 82% Analysis Date = 05/23/15 Pct Recovery = 82% Analysis Date = 05/22/15 Pct Recovery = 82% Analysis Date = 05/22/15 Pct Recovery = 82% Analysis Date = 05/20/15 Pct Recovery = 82% Analysis Date = 05/20/15 Pct Recovery = 82% Analysis Date = 05/18/15 Pct Recovery = 81% Analysis Date = 05/18/15 Pct Recovery = 81% Analysis Date = 05/17/15 Pct Recovery = 81% Analysis Date = 05/17/15 Pct Recovery = 81% Analysis Date = 05/15/15 Pct Recovery = 81% Analysis Date = 05/15/15 Pct Recovery = 81% Analysis Date = 05/13/15 Pct Recovery = 81% Analysis Date = 05/13/15 Pct Recovery = 81% Analysis Date = 05/12/15 Pct Recovery = 80% Analysis Date = 05/12/15 Pct Recovery = 80% Analysis Date = 05/10/15 Pct Recovery = 80% Analysis Date = 05/10/15 Pct Recovery = 80% Analysis Date = 05/09/15 Pct Recovery = 80% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
BUTANE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 16 81% 16% 80% 21%
Total 16 81% 16% 80% 21%

Sample Statistics
BUTANE

Characteristic N % % Basis
Plotted 16 94% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 17 .  
False Negatives 1 6% 1 out of 17
Not Spiked 47 .  
False Positives 0 0% 0 out of 47

BQS OBSP Determination:
BUTYLBENZENE
METHOD: 4440 , TESTIDCODE: 77342GCM66
Open Data Set

Analysis Date = 12/16/16 SpikeMix = NSI 041816AVOC: 40 µl & ChemService 5082900: 40 µl Pct Recovery = 89% Analysis Date = 08/04/16 SpikeMix = Crescent 03FF058: 40 µl & Supelco LC20141V: 40 µl Pct Recovery = 79% Analysis Date = 07/20/16 SpikeMix = Supelco LC20141V: 40 µl & Accu 216041125: 40 µl Pct Recovery = 96% Analysis Date = 08/26/16 SpikeMix = NSI 041816AVOC: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 79% Analysis Date = 08/12/16 SpikeMix = ChemService 5082900: 25 µl & Phenova B20160319: 25 µl Pct Recovery = 79% Analysis Date = 06/30/16 SpikeMix = Crescent 03FF058: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 74% Analysis Date = 11/21/16 SpikeMix = Crescent 03FF058: 25 µl & Supelco LC20141V: 25 µl Pct Recovery = 82% Analysis Date = 09/08/16 SpikeMix = Supelco LC20141V: 25 µl & Accu 216041125: 25 µl Pct Recovery = 79% Analysis Date = 04/09/15 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 80% Analysis Date = 03/06/15 SpikeMix = ERA 0227-14-06.1A: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 77% Analysis Date = 11/14/14 SpikeMix = Crescent 03DD004: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 68% Analysis Date = 08/16/14 SpikeMix = ERA 0227-14-06.1A: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 71% Analysis Date = 07/01/14 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 81% Analysis Date = 11/22/14 SpikeMix = NSI 032614: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 75% Analysis Date = 06/10/14 SpikeMix = Crescent 03DD004: 20 µl & NSI 032614: 20 µl Pct Recovery = 66% Analysis Date = 06/10/14 SpikeMix = NSI 032614: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 78% Analysis Date = 05/01/14 SpikeMix = Accu 214031115: 20 µl & NSI 032614: 20 µl Pct Recovery = 64% Analysis Date = 08/15/15 SpikeMix = Supelco LC13545: 25 µl & Crescent 04EE008: 25 µl Pct Recovery = 91% Analysis Date = 06/16/15 SpikeMix = ERA 0406-15-03: 25 µl & Supelco LC13545: 25 µl Pct Recovery = 84% Analysis Date = 11/29/16 SpikeMix = ChemService 5082900: 15 µl & Phenova B20160319: 15 µl Pct Recovery = 80% Analysis Date = 09/28/16 SpikeMix = Crescent 03FF058: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 68% Analysis Date = 06/30/16 SpikeMix = ChemService 5082900: 15 µl & Accu 216041125: 15 µl Pct Recovery = 75% Analysis Date = 06/10/16 SpikeMix = NSI 041816AVOC: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 86% Analysis Date = 10/13/16 SpikeMix = NSI 041816AVOC: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 73% Analysis Date = 05/27/16 SpikeMix = Phenova B20160319: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 82% Analysis Date = 04/26/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 71% Analysis Date = 04/02/16 SpikeMix = Supelco LC13545: 15 µl & Accu 215041380: 15 µl Pct Recovery = 75% Analysis Date = 02/05/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 85% Analysis Date = 12/18/15 SpikeMix = Supelco LC13545: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 78% Analysis Date = 11/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 97% Analysis Date = 10/16/15 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 85% Analysis Date = 05/09/15 SpikeMix = Spex Organics EN150428007: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 82% Analysis Date = 01/13/15 SpikeMix = Accu 214031115: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 74% Analysis Date = 10/21/14 SpikeMix = ERA 0227-14-06.1A: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 75% Analysis Date = 10/04/14 SpikeMix = Crescent 03DD004: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 74% Analysis Date = 07/11/14 SpikeMix = Spex Organics C1140417015: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 77% Analysis Date = 09/09/14 SpikeMix = Accu 214031115: 10 µl & NSI 032614: 10 µl Pct Recovery = 93% Analysis Date = 09/09/14 SpikeMix = NSI 032614: 10 µl & Spex Organics C1140417015: 10 µl Pct Recovery = 91% Analysis Date = 07/29/14 SpikeMix = Crescent 03DD004: 10 µl & NSI 032614: 10 µl Pct Recovery = 75% Analysis Date = 05/30/14 SpikeMix = NSI 032614: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 59% Analysis Date = 05/13/16 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 79% Analysis Date = 03/17/16 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 70% Analysis Date = 02/18/16 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 85% Analysis Date = 12/10/15 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 93% Analysis Date = 11/12/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 103% Analysis Date = 09/03/15 SpikeMix = NSI 050515AVOC: 10 µl & Spex Organics EN150428007: 10 µl Pct Recovery = 76% Analysis Date = 06/27/15 SpikeMix = ERA 0406-15-03: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 82% Analysis Date = 05/21/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 82% Analysis Date = 05/09/15 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 81% Analysis Date = 12/15/16 Pct Recovery = 78% Analysis Date = 12/11/16 Pct Recovery = 78% Analysis Date = 12/11/16 Pct Recovery = 78% Analysis Date = 12/06/16 Pct Recovery = 78% Analysis Date = 12/06/16 Pct Recovery = 78% Analysis Date = 12/01/16 Pct Recovery = 79% Analysis Date = 12/01/16 Pct Recovery = 79% Analysis Date = 11/26/16 Pct Recovery = 79% Analysis Date = 11/26/16 Pct Recovery = 79% Analysis Date = 11/21/16 Pct Recovery = 79% Analysis Date = 11/21/16 Pct Recovery = 79% Analysis Date = 11/17/16 Pct Recovery = 79% Analysis Date = 11/17/16 Pct Recovery = 79% Analysis Date = 11/12/16 Pct Recovery = 79% Analysis Date = 11/12/16 Pct Recovery = 79% Analysis Date = 11/07/16 Pct Recovery = 79% Analysis Date = 11/07/16 Pct Recovery = 79% Analysis Date = 11/02/16 Pct Recovery = 79% Analysis Date = 11/02/16 Pct Recovery = 79% Analysis Date = 10/28/16 Pct Recovery = 79% Analysis Date = 10/28/16 Pct Recovery = 79% Analysis Date = 10/24/16 Pct Recovery = 79% Analysis Date = 10/24/16 Pct Recovery = 79% Analysis Date = 10/19/16 Pct Recovery = 79% Analysis Date = 10/19/16 Pct Recovery = 79% Analysis Date = 10/14/16 Pct Recovery = 79% Analysis Date = 10/14/16 Pct Recovery = 79% Analysis Date = 10/09/16 Pct Recovery = 79% Analysis Date = 10/09/16 Pct Recovery = 79% Analysis Date = 10/04/16 Pct Recovery = 79% Analysis Date = 10/04/16 Pct Recovery = 79% Analysis Date = 09/30/16 Pct Recovery = 79% Analysis Date = 09/30/16 Pct Recovery = 79% Analysis Date = 09/25/16 Pct Recovery = 79% Analysis Date = 09/25/16 Pct Recovery = 79% Analysis Date = 09/20/16 Pct Recovery = 79% Analysis Date = 09/20/16 Pct Recovery = 79% Analysis Date = 09/15/16 Pct Recovery = 79% Analysis Date = 09/15/16 Pct Recovery = 79% Analysis Date = 09/10/16 Pct Recovery = 79% Analysis Date = 09/10/16 Pct Recovery = 79% Analysis Date = 09/06/16 Pct Recovery = 79% Analysis Date = 09/06/16 Pct Recovery = 79% Analysis Date = 09/01/16 Pct Recovery = 79% Analysis Date = 09/01/16 Pct Recovery = 79% Analysis Date = 08/27/16 Pct Recovery = 79% Analysis Date = 08/27/16 Pct Recovery = 79% Analysis Date = 08/22/16 Pct Recovery = 79% Analysis Date = 08/22/16 Pct Recovery = 79% Analysis Date = 08/17/16 Pct Recovery = 79% Analysis Date = 08/17/16 Pct Recovery = 79% Analysis Date = 08/13/16 Pct Recovery = 80% Analysis Date = 08/13/16 Pct Recovery = 80% Analysis Date = 08/08/16 Pct Recovery = 80% Analysis Date = 08/08/16 Pct Recovery = 80% Analysis Date = 08/03/16 Pct Recovery = 80% Analysis Date = 08/03/16 Pct Recovery = 80% Analysis Date = 07/29/16 Pct Recovery = 80% Analysis Date = 07/29/16 Pct Recovery = 80% Analysis Date = 07/24/16 Pct Recovery = 80% Analysis Date = 07/24/16 Pct Recovery = 80% Analysis Date = 07/20/16 Pct Recovery = 80% Analysis Date = 07/20/16 Pct Recovery = 80% Analysis Date = 07/15/16 Pct Recovery = 80% Analysis Date = 07/15/16 Pct Recovery = 80% Analysis Date = 07/10/16 Pct Recovery = 80% Analysis Date = 07/10/16 Pct Recovery = 80% Analysis Date = 07/05/16 Pct Recovery = 80% Analysis Date = 07/05/16 Pct Recovery = 80% Analysis Date = 06/30/16 Pct Recovery = 80% Analysis Date = 06/30/16 Pct Recovery = 80% Analysis Date = 06/26/16 Pct Recovery = 80% Analysis Date = 06/26/16 Pct Recovery = 80% Analysis Date = 06/21/16 Pct Recovery = 80% Analysis Date = 06/21/16 Pct Recovery = 80% Analysis Date = 06/16/16 Pct Recovery = 80% Analysis Date = 06/16/16 Pct Recovery = 80% Analysis Date = 06/11/16 Pct Recovery = 80% Analysis Date = 06/11/16 Pct Recovery = 80% Analysis Date = 06/06/16 Pct Recovery = 81% Analysis Date = 06/06/16 Pct Recovery = 81% Analysis Date = 06/02/16 Pct Recovery = 81% Analysis Date = 06/02/16 Pct Recovery = 81% Analysis Date = 05/28/16 Pct Recovery = 81% Analysis Date = 05/28/16 Pct Recovery = 81% Analysis Date = 05/23/16 Pct Recovery = 81% Analysis Date = 05/23/16 Pct Recovery = 81% Analysis Date = 05/18/16 Pct Recovery = 81% Analysis Date = 05/18/16 Pct Recovery = 81% Analysis Date = 05/13/16 Pct Recovery = 81% Analysis Date = 05/13/16 Pct Recovery = 81% Analysis Date = 05/09/16 Pct Recovery = 81% Analysis Date = 05/09/16 Pct Recovery = 81% Analysis Date = 05/04/16 Pct Recovery = 81% Analysis Date = 05/04/16 Pct Recovery = 81% Analysis Date = 04/29/16 Pct Recovery = 81% Analysis Date = 04/29/16 Pct Recovery = 81% Analysis Date = 04/24/16 Pct Recovery = 81% Analysis Date = 04/24/16 Pct Recovery = 81% Analysis Date = 04/19/16 Pct Recovery = 82% Analysis Date = 04/19/16 Pct Recovery = 82% Analysis Date = 04/15/16 Pct Recovery = 82% Analysis Date = 04/15/16 Pct Recovery = 82% Analysis Date = 04/10/16 Pct Recovery = 82% Analysis Date = 04/10/16 Pct Recovery = 82% Analysis Date = 04/05/16 Pct Recovery = 82% Analysis Date = 04/05/16 Pct Recovery = 82% Analysis Date = 03/31/16 Pct Recovery = 82% Analysis Date = 03/31/16 Pct Recovery = 82% Analysis Date = 03/26/16 Pct Recovery = 82% Analysis Date = 03/26/16 Pct Recovery = 82% Analysis Date = 03/22/16 Pct Recovery = 82% Analysis Date = 03/22/16 Pct Recovery = 82% Analysis Date = 03/17/16 Pct Recovery = 83% Analysis Date = 03/17/16 Pct Recovery = 83% Analysis Date = 03/12/16 Pct Recovery = 83% Analysis Date = 03/12/16 Pct Recovery = 83% Analysis Date = 03/07/16 Pct Recovery = 83% Analysis Date = 03/07/16 Pct Recovery = 83% Analysis Date = 03/02/16 Pct Recovery = 83% Analysis Date = 03/02/16 Pct Recovery = 83% Analysis Date = 02/27/16 Pct Recovery = 83% Analysis Date = 02/27/16 Pct Recovery = 83% Analysis Date = 02/22/16 Pct Recovery = 83% Analysis Date = 02/22/16 Pct Recovery = 83% Analysis Date = 02/17/16 Pct Recovery = 83% Analysis Date = 02/17/16 Pct Recovery = 83% Analysis Date = 02/12/16 Pct Recovery = 83% Analysis Date = 02/12/16 Pct Recovery = 83% Analysis Date = 02/07/16 Pct Recovery = 83% Analysis Date = 02/07/16 Pct Recovery = 83% Analysis Date = 02/03/16 Pct Recovery = 84% Analysis Date = 02/03/16 Pct Recovery = 84% Analysis Date = 01/29/16 Pct Recovery = 84% Analysis Date = 01/29/16 Pct Recovery = 84% Analysis Date = 01/24/16 Pct Recovery = 84% Analysis Date = 01/24/16 Pct Recovery = 84% Analysis Date = 01/19/16 Pct Recovery = 84% Analysis Date = 01/19/16 Pct Recovery = 84% Analysis Date = 01/14/16 Pct Recovery = 84% Analysis Date = 01/14/16 Pct Recovery = 84% Analysis Date = 01/10/16 Pct Recovery = 84% Analysis Date = 01/10/16 Pct Recovery = 84% Analysis Date = 01/05/16 Pct Recovery = 84% Analysis Date = 01/05/16 Pct Recovery = 84% Analysis Date = 12/31/15 Pct Recovery = 84% Analysis Date = 12/31/15 Pct Recovery = 84% Analysis Date = 12/26/15 Pct Recovery = 84% Analysis Date = 12/26/15 Pct Recovery = 84% Analysis Date = 12/21/15 Pct Recovery = 84% Analysis Date = 12/21/15 Pct Recovery = 84% Analysis Date = 12/17/15 Pct Recovery = 84% Analysis Date = 12/17/15 Pct Recovery = 84% Analysis Date = 12/12/15 Pct Recovery = 84% Analysis Date = 12/12/15 Pct Recovery = 84% Analysis Date = 12/07/15 Pct Recovery = 84% Analysis Date = 12/07/15 Pct Recovery = 84% Analysis Date = 12/02/15 Pct Recovery = 84% Analysis Date = 12/02/15 Pct Recovery = 84% Analysis Date = 11/27/15 Pct Recovery = 84% Analysis Date = 11/27/15 Pct Recovery = 84% Analysis Date = 11/23/15 Pct Recovery = 84% Analysis Date = 11/23/15 Pct Recovery = 84% Analysis Date = 11/18/15 Pct Recovery = 84% Analysis Date = 11/18/15 Pct Recovery = 84% Analysis Date = 11/13/15 Pct Recovery = 84% Analysis Date = 11/13/15 Pct Recovery = 84% Analysis Date = 11/08/15 Pct Recovery = 84% Analysis Date = 11/08/15 Pct Recovery = 84% Analysis Date = 11/03/15 Pct Recovery = 84% Analysis Date = 11/03/15 Pct Recovery = 84% Analysis Date = 10/30/15 Pct Recovery = 84% Analysis Date = 10/30/15 Pct Recovery = 84% Analysis Date = 10/25/15 Pct Recovery = 84% Analysis Date = 10/25/15 Pct Recovery = 84% Analysis Date = 10/20/15 Pct Recovery = 84% Analysis Date = 10/20/15 Pct Recovery = 84% Analysis Date = 10/15/15 Pct Recovery = 84% Analysis Date = 10/15/15 Pct Recovery = 84% Analysis Date = 10/10/15 Pct Recovery = 84% Analysis Date = 10/10/15 Pct Recovery = 84% Analysis Date = 10/06/15 Pct Recovery = 84% Analysis Date = 10/06/15 Pct Recovery = 84% Analysis Date = 10/01/15 Pct Recovery = 84% Analysis Date = 10/01/15 Pct Recovery = 84% Analysis Date = 09/26/15 Pct Recovery = 84% Analysis Date = 09/26/15 Pct Recovery = 84% Analysis Date = 09/21/15 Pct Recovery = 84% Analysis Date = 09/21/15 Pct Recovery = 84% Analysis Date = 09/16/15 Pct Recovery = 84% Analysis Date = 09/16/15 Pct Recovery = 84% Analysis Date = 09/12/15 Pct Recovery = 84% Analysis Date = 09/12/15 Pct Recovery = 84% Analysis Date = 09/07/15 Pct Recovery = 84% Analysis Date = 09/07/15 Pct Recovery = 84% Analysis Date = 09/02/15 Pct Recovery = 84% Analysis Date = 09/02/15 Pct Recovery = 84% Analysis Date = 08/28/15 Pct Recovery = 84% Analysis Date = 08/28/15 Pct Recovery = 84% Analysis Date = 08/23/15 Pct Recovery = 83% Analysis Date = 08/23/15 Pct Recovery = 83% Analysis Date = 08/19/15 Pct Recovery = 83% Analysis Date = 08/19/15 Pct Recovery = 83% Analysis Date = 08/14/15 Pct Recovery = 83% Analysis Date = 08/14/15 Pct Recovery = 83% Analysis Date = 08/09/15 Pct Recovery = 83% Analysis Date = 08/09/15 Pct Recovery = 83% Analysis Date = 08/04/15 Pct Recovery = 83% Analysis Date = 08/04/15 Pct Recovery = 83% Analysis Date = 07/30/15 Pct Recovery = 83% Analysis Date = 07/30/15 Pct Recovery = 83% Analysis Date = 07/26/15 Pct Recovery = 83% Analysis Date = 07/26/15 Pct Recovery = 83% Analysis Date = 07/21/15 Pct Recovery = 83% Analysis Date = 07/21/15 Pct Recovery = 83% Analysis Date = 07/16/15 Pct Recovery = 83% Analysis Date = 07/16/15 Pct Recovery = 83% Analysis Date = 07/11/15 Pct Recovery = 83% Analysis Date = 07/11/15 Pct Recovery = 83% Analysis Date = 07/06/15 Pct Recovery = 83% Analysis Date = 07/06/15 Pct Recovery = 83% Analysis Date = 07/02/15 Pct Recovery = 83% Analysis Date = 07/02/15 Pct Recovery = 83% Analysis Date = 06/27/15 Pct Recovery = 83% Analysis Date = 06/27/15 Pct Recovery = 83% Analysis Date = 06/22/15 Pct Recovery = 83% Analysis Date = 06/22/15 Pct Recovery = 83% Analysis Date = 06/17/15 Pct Recovery = 83% Analysis Date = 06/17/15 Pct Recovery = 83% Analysis Date = 06/12/15 Pct Recovery = 83% Analysis Date = 06/12/15 Pct Recovery = 83% Analysis Date = 06/08/15 Pct Recovery = 82% Analysis Date = 06/08/15 Pct Recovery = 82% Analysis Date = 06/03/15 Pct Recovery = 82% Analysis Date = 06/03/15 Pct Recovery = 82% Analysis Date = 05/29/15 Pct Recovery = 82% Analysis Date = 05/29/15 Pct Recovery = 82% Analysis Date = 05/24/15 Pct Recovery = 82% Analysis Date = 05/24/15 Pct Recovery = 82% Analysis Date = 05/19/15 Pct Recovery = 82% Analysis Date = 05/19/15 Pct Recovery = 82% Analysis Date = 05/15/15 Pct Recovery = 82% Analysis Date = 05/15/15 Pct Recovery = 82% Analysis Date = 05/10/15 Pct Recovery = 82% Analysis Date = 05/10/15 Pct Recovery = 82% Analysis Date = 05/05/15 Pct Recovery = 82% Analysis Date = 05/05/15 Pct Recovery = 82% Analysis Date = 04/30/15 Pct Recovery = 82% Analysis Date = 04/30/15 Pct Recovery = 82% Analysis Date = 04/25/15 Pct Recovery = 81% Analysis Date = 04/25/15 Pct Recovery = 81% Analysis Date = 04/21/15 Pct Recovery = 81% Analysis Date = 04/21/15 Pct Recovery = 81% Analysis Date = 04/16/15 Pct Recovery = 81% Analysis Date = 04/16/15 Pct Recovery = 81% Analysis Date = 04/11/15 Pct Recovery = 81% Analysis Date = 04/11/15 Pct Recovery = 81% Analysis Date = 04/06/15 Pct Recovery = 81% Analysis Date = 04/06/15 Pct Recovery = 81% Analysis Date = 04/01/15 Pct Recovery = 81% Analysis Date = 04/01/15 Pct Recovery = 81% Analysis Date = 03/28/15 Pct Recovery = 81% Analysis Date = 03/28/15 Pct Recovery = 81% Analysis Date = 03/23/15 Pct Recovery = 80% Analysis Date = 03/23/15 Pct Recovery = 80% Analysis Date = 03/18/15 Pct Recovery = 80% Analysis Date = 03/18/15 Pct Recovery = 80% Analysis Date = 03/13/15 Pct Recovery = 80% Analysis Date = 03/13/15 Pct Recovery = 80% Analysis Date = 03/08/15 Pct Recovery = 80% Analysis Date = 03/08/15 Pct Recovery = 80% Analysis Date = 03/04/15 Pct Recovery = 80% Analysis Date = 03/04/15 Pct Recovery = 80% Analysis Date = 02/27/15 Pct Recovery = 80% Analysis Date = 02/27/15 Pct Recovery = 80% Analysis Date = 02/22/15 Pct Recovery = 80% Analysis Date = 02/22/15 Pct Recovery = 80% Analysis Date = 02/17/15 Pct Recovery = 79% Analysis Date = 02/17/15 Pct Recovery = 79% Analysis Date = 02/12/15 Pct Recovery = 79% Analysis Date = 02/12/15 Pct Recovery = 79% Analysis Date = 02/08/15 Pct Recovery = 79% Analysis Date = 02/08/15 Pct Recovery = 79% Analysis Date = 02/03/15 Pct Recovery = 79% Analysis Date = 02/03/15 Pct Recovery = 79% Analysis Date = 01/29/15 Pct Recovery = 79% Analysis Date = 01/29/15 Pct Recovery = 79% Analysis Date = 01/24/15 Pct Recovery = 79% Analysis Date = 01/24/15 Pct Recovery = 79% Analysis Date = 01/19/15 Pct Recovery = 79% Analysis Date = 01/19/15 Pct Recovery = 79% Analysis Date = 01/15/15 Pct Recovery = 79% Analysis Date = 01/15/15 Pct Recovery = 79% Analysis Date = 01/10/15 Pct Recovery = 79% Analysis Date = 01/10/15 Pct Recovery = 79% Analysis Date = 01/05/15 Pct Recovery = 78% Analysis Date = 01/05/15 Pct Recovery = 78% Analysis Date = 12/31/14 Pct Recovery = 78% Analysis Date = 12/31/14 Pct Recovery = 78% Analysis Date = 12/26/14 Pct Recovery = 78% Analysis Date = 12/26/14 Pct Recovery = 78% Analysis Date = 12/22/14 Pct Recovery = 78% Analysis Date = 12/22/14 Pct Recovery = 78% Analysis Date = 12/17/14 Pct Recovery = 78% Analysis Date = 12/17/14 Pct Recovery = 78% Analysis Date = 12/12/14 Pct Recovery = 78% Analysis Date = 12/12/14 Pct Recovery = 78% Analysis Date = 12/07/14 Pct Recovery = 78% Analysis Date = 12/07/14 Pct Recovery = 78% Analysis Date = 12/02/14 Pct Recovery = 78% Analysis Date = 12/02/14 Pct Recovery = 78% Analysis Date = 11/28/14 Pct Recovery = 77% Analysis Date = 11/28/14 Pct Recovery = 77% Analysis Date = 11/23/14 Pct Recovery = 77% Analysis Date = 11/23/14 Pct Recovery = 77% Analysis Date = 11/18/14 Pct Recovery = 77% Analysis Date = 11/18/14 Pct Recovery = 77% Analysis Date = 11/13/14 Pct Recovery = 77% Analysis Date = 11/13/14 Pct Recovery = 77% Analysis Date = 11/08/14 Pct Recovery = 77% Analysis Date = 11/08/14 Pct Recovery = 77% Analysis Date = 11/04/14 Pct Recovery = 77% Analysis Date = 11/04/14 Pct Recovery = 77% Analysis Date = 10/30/14 Pct Recovery = 77% Analysis Date = 10/30/14 Pct Recovery = 77% Analysis Date = 10/25/14 Pct Recovery = 77% Analysis Date = 10/25/14 Pct Recovery = 77% Analysis Date = 10/20/14 Pct Recovery = 76% Analysis Date = 10/20/14 Pct Recovery = 76% Analysis Date = 10/15/14 Pct Recovery = 76% Analysis Date = 10/15/14 Pct Recovery = 76% Analysis Date = 10/11/14 Pct Recovery = 76% Analysis Date = 10/11/14 Pct Recovery = 76% Analysis Date = 10/06/14 Pct Recovery = 76% Analysis Date = 10/06/14 Pct Recovery = 76% Analysis Date = 10/01/14 Pct Recovery = 76% Analysis Date = 10/01/14 Pct Recovery = 76% Analysis Date = 09/26/14 Pct Recovery = 76% Analysis Date = 09/26/14 Pct Recovery = 76% Analysis Date = 09/21/14 Pct Recovery = 76% Analysis Date = 09/21/14 Pct Recovery = 76% Analysis Date = 09/17/14 Pct Recovery = 75% Analysis Date = 09/17/14 Pct Recovery = 75% Analysis Date = 09/12/14 Pct Recovery = 75% Analysis Date = 09/12/14 Pct Recovery = 75% Analysis Date = 09/07/14 Pct Recovery = 75% Analysis Date = 09/07/14 Pct Recovery = 75% Analysis Date = 09/02/14 Pct Recovery = 75% Analysis Date = 09/02/14 Pct Recovery = 75% Analysis Date = 08/28/14 Pct Recovery = 75% Analysis Date = 08/28/14 Pct Recovery = 75% Analysis Date = 08/24/14 Pct Recovery = 75% Analysis Date = 08/24/14 Pct Recovery = 75% Analysis Date = 08/19/14 Pct Recovery = 75% Analysis Date = 08/19/14 Pct Recovery = 75% Analysis Date = 08/14/14 Pct Recovery = 75% Analysis Date = 08/14/14 Pct Recovery = 75% Analysis Date = 08/09/14 Pct Recovery = 74% Analysis Date = 08/09/14 Pct Recovery = 74% Analysis Date = 08/04/14 Pct Recovery = 74% Analysis Date = 08/04/14 Pct Recovery = 74% Analysis Date = 07/31/14 Pct Recovery = 74% Analysis Date = 07/31/14 Pct Recovery = 74% Analysis Date = 07/26/14 Pct Recovery = 74% Analysis Date = 07/26/14 Pct Recovery = 74% Analysis Date = 07/21/14 Pct Recovery = 74% Analysis Date = 07/21/14 Pct Recovery = 74% Analysis Date = 07/16/14 Pct Recovery = 74% Analysis Date = 07/16/14 Pct Recovery = 74% Analysis Date = 07/11/14 Pct Recovery = 74% Analysis Date = 07/11/14 Pct Recovery = 74% Analysis Date = 07/07/14 Pct Recovery = 74% Analysis Date = 07/07/14 Pct Recovery = 74% Analysis Date = 07/02/14 Pct Recovery = 73% Analysis Date = 07/02/14 Pct Recovery = 73% Analysis Date = 06/27/14 Pct Recovery = 73% Analysis Date = 06/27/14 Pct Recovery = 73% Analysis Date = 06/22/14 Pct Recovery = 73% Analysis Date = 06/22/14 Pct Recovery = 73% Analysis Date = 06/17/14 Pct Recovery = 73% Analysis Date = 06/17/14 Pct Recovery = 73% Analysis Date = 06/13/14 Pct Recovery = 73% Analysis Date = 06/13/14 Pct Recovery = 73% Analysis Date = 06/08/14 Pct Recovery = 73% Analysis Date = 06/08/14 Pct Recovery = 73% Analysis Date = 06/03/14 Pct Recovery = 73% Analysis Date = 06/03/14 Pct Recovery = 73% Analysis Date = 05/29/14 Pct Recovery = 73% Analysis Date = 05/29/14 Pct Recovery = 73% Analysis Date = 05/24/14 Pct Recovery = 72% Analysis Date = 05/24/14 Pct Recovery = 72% Analysis Date = 05/20/14 Pct Recovery = 72% Analysis Date = 05/20/14 Pct Recovery = 72% Analysis Date = 05/15/14 Pct Recovery = 72% Analysis Date = 05/15/14 Pct Recovery = 72% Analysis Date = 05/10/14 Pct Recovery = 72% Analysis Date = 05/10/14 Pct Recovery = 72% Analysis Date = 05/05/14 Pct Recovery = 72% Analysis Date = 05/05/14 Pct Recovery = 72% Analysis Date = 05/01/14 Pct Recovery = 72% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
BUTYLBENZENE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 49 80% 9% 79% 7%
Total 49 80% 9% 79% 7%

Sample Statistics
BUTYLBENZENE

Characteristic N % % Basis
Plotted 49 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 49 .  
False Negatives 0 0% 0 out of 49
Not Spiked 24 .  
False Positives 0 0% 0 out of 24

BQS OBSP Determination:
CARBON DISULFIDE
METHOD: 4440 , TESTIDCODE: 77041GCM66
Open Data Set

Analysis Date = 12/16/16 SpikeMix = NSI 041816AVOC: 40 µl & ChemService 5082900: 40 µl Pct Recovery = 102% Analysis Date = 08/04/16 SpikeMix = Crescent 03FF058: 40 µl & Supelco LC20141V: 40 µl Pct Recovery = 93% Analysis Date = 07/20/16 SpikeMix = Supelco LC20141V: 40 µl & Accu 216041125: 40 µl Pct Recovery = 96% Analysis Date = 08/26/16 SpikeMix = NSI 041816AVOC: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 97% Analysis Date = 08/12/16 SpikeMix = ChemService 5082900: 25 µl & Phenova B20160319: 25 µl Pct Recovery = 96% Analysis Date = 06/30/16 SpikeMix = Crescent 03FF058: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 99% Analysis Date = 11/21/16 SpikeMix = Crescent 03FF058: 25 µl & Supelco LC20141V: 25 µl Pct Recovery = 86% Analysis Date = 09/08/16 SpikeMix = Supelco LC20141V: 25 µl & Accu 216041125: 25 µl Pct Recovery = 95% Analysis Date = 04/09/15 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 70% Analysis Date = 03/06/15 SpikeMix = ERA 0227-14-06.1A: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 88% Analysis Date = 11/22/14 SpikeMix = NSI 032614: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 115% Analysis Date = 11/14/14 SpikeMix = Crescent 03DD004: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 83% Analysis Date = 08/16/14 SpikeMix = ERA 0227-14-06.1A: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 105% Analysis Date = 07/01/14 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 115% Analysis Date = 06/10/14 SpikeMix = Crescent 03DD004: 20 µl & NSI 032614: 20 µl Pct Recovery = 148% Analysis Date = 06/10/14 SpikeMix = NSI 032614: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 159% Analysis Date = 05/01/14 SpikeMix = Accu 214031115: 20 µl & NSI 032614: 20 µl Pct Recovery = 125% Analysis Date = 09/29/15 SpikeMix = Accu 215041380: 25 µl & ERA 0406-15-03: 25 µl Pct Recovery = 117% Analysis Date = 06/16/15 SpikeMix = ERA 0406-15-03: 25 µl & Supelco LC13545: 25 µl Pct Recovery = 107% Analysis Date = 07/13/15 SpikeMix = Crescent 04EE008: 25 µl & NSI 050515AVOC: 25 µl Pct Recovery = 108% Analysis Date = 11/29/16 SpikeMix = ChemService 5082900: 15 µl & Phenova B20160319: 15 µl Pct Recovery = 98% Analysis Date = 09/28/16 SpikeMix = Crescent 03FF058: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 100% Analysis Date = 06/30/16 SpikeMix = ChemService 5082900: 15 µl & Accu 216041125: 15 µl Pct Recovery = 106% Analysis Date = 06/10/16 SpikeMix = NSI 041816AVOC: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 87% Analysis Date = 10/13/16 SpikeMix = NSI 041816AVOC: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 99% Analysis Date = 05/27/16 SpikeMix = Phenova B20160319: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 90% Analysis Date = 04/26/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 108% Analysis Date = 03/04/16 SpikeMix = Accu 215041380: 15 µl & ERA 0406-15-03: 15 µl Pct Recovery = 152% Analysis Date = 02/05/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 107% Analysis Date = 10/16/15 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 123% Analysis Date = 11/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 112% Analysis Date = 10/17/15 SpikeMix = Crescent 04EE008: 15 µl & NSI 050515AVOC: 15 µl Pct Recovery = 106% Analysis Date = 06/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Accu 215041380: 15 µl Pct Recovery = 112% Analysis Date = 01/13/15 SpikeMix = Accu 214031115: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 93% Analysis Date = 10/21/14 SpikeMix = ERA 0227-14-06.1A: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 89% Analysis Date = 10/04/14 SpikeMix = Crescent 03DD004: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 86% Analysis Date = 09/09/14 SpikeMix = Accu 214031115: 10 µl & NSI 032614: 10 µl Pct Recovery = 140% Analysis Date = 09/09/14 SpikeMix = NSI 032614: 10 µl & Spex Organics C1140417015: 10 µl Pct Recovery = 140% Analysis Date = 07/29/14 SpikeMix = Crescent 03DD004: 10 µl & NSI 032614: 10 µl Pct Recovery = 151% Analysis Date = 07/11/14 SpikeMix = Spex Organics C1140417015: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 102% Analysis Date = 11/20/15 SpikeMix = Accu 215041380: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 122% Analysis Date = 07/31/15 SpikeMix = Crescent 04EE008: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 111% Analysis Date = 06/27/15 SpikeMix = ERA 0406-15-03: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 122% Analysis Date = 03/17/16 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 154% Analysis Date = 01/27/16 SpikeMix = Crescent 04EE008: 10 µl & NSI 050515AVOC: 10 µl Pct Recovery = 119% Analysis Date = 12/10/15 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 128% Analysis Date = 09/03/15 SpikeMix = NSI 050515AVOC: 10 µl & Spex Organics EN150428007: 10 µl Pct Recovery = 116% Analysis Date = 12/15/16 Pct Recovery = 89% Analysis Date = 12/11/16 Pct Recovery = 89% Analysis Date = 12/11/16 Pct Recovery = 89% Analysis Date = 12/06/16 Pct Recovery = 90% Analysis Date = 12/06/16 Pct Recovery = 90% Analysis Date = 12/01/16 Pct Recovery = 90% Analysis Date = 12/01/16 Pct Recovery = 90% Analysis Date = 11/26/16 Pct Recovery = 91% Analysis Date = 11/26/16 Pct Recovery = 91% Analysis Date = 11/21/16 Pct Recovery = 91% Analysis Date = 11/21/16 Pct Recovery = 91% Analysis Date = 11/17/16 Pct Recovery = 92% Analysis Date = 11/17/16 Pct Recovery = 92% Analysis Date = 11/12/16 Pct Recovery = 92% Analysis Date = 11/12/16 Pct Recovery = 92% Analysis Date = 11/07/16 Pct Recovery = 93% Analysis Date = 11/07/16 Pct Recovery = 93% Analysis Date = 11/02/16 Pct Recovery = 93% Analysis Date = 11/02/16 Pct Recovery = 93% Analysis Date = 10/28/16 Pct Recovery = 93% Analysis Date = 10/28/16 Pct Recovery = 93% Analysis Date = 10/24/16 Pct Recovery = 94% Analysis Date = 10/24/16 Pct Recovery = 94% Analysis Date = 10/19/16 Pct Recovery = 94% Analysis Date = 10/19/16 Pct Recovery = 94% Analysis Date = 10/14/16 Pct Recovery = 95% Analysis Date = 10/14/16 Pct Recovery = 95% Analysis Date = 10/09/16 Pct Recovery = 95% Analysis Date = 10/09/16 Pct Recovery = 95% Analysis Date = 10/04/16 Pct Recovery = 96% Analysis Date = 10/04/16 Pct Recovery = 96% Analysis Date = 09/30/16 Pct Recovery = 96% Analysis Date = 09/30/16 Pct Recovery = 96% Analysis Date = 09/25/16 Pct Recovery = 96% Analysis Date = 09/25/16 Pct Recovery = 96% Analysis Date = 09/20/16 Pct Recovery = 97% Analysis Date = 09/20/16 Pct Recovery = 97% Analysis Date = 09/15/16 Pct Recovery = 97% Analysis Date = 09/15/16 Pct Recovery = 97% Analysis Date = 09/10/16 Pct Recovery = 98% Analysis Date = 09/10/16 Pct Recovery = 98% Analysis Date = 09/06/16 Pct Recovery = 98% Analysis Date = 09/06/16 Pct Recovery = 98% Analysis Date = 09/01/16 Pct Recovery = 99% Analysis Date = 09/01/16 Pct Recovery = 99% Analysis Date = 08/27/16 Pct Recovery = 99% Analysis Date = 08/27/16 Pct Recovery = 99% Analysis Date = 08/22/16 Pct Recovery = 99% Analysis Date = 08/22/16 Pct Recovery = 99% Analysis Date = 08/17/16 Pct Recovery = 100% Analysis Date = 08/17/16 Pct Recovery = 100% Analysis Date = 08/13/16 Pct Recovery = 100% Analysis Date = 08/13/16 Pct Recovery = 100% Analysis Date = 08/08/16 Pct Recovery = 101% Analysis Date = 08/08/16 Pct Recovery = 101% Analysis Date = 08/03/16 Pct Recovery = 101% Analysis Date = 08/03/16 Pct Recovery = 101% Analysis Date = 07/29/16 Pct Recovery = 102% Analysis Date = 07/29/16 Pct Recovery = 102% Analysis Date = 07/24/16 Pct Recovery = 102% Analysis Date = 07/24/16 Pct Recovery = 102% Analysis Date = 07/20/16 Pct Recovery = 103% Analysis Date = 07/20/16 Pct Recovery = 103% Analysis Date = 07/15/16 Pct Recovery = 103% Analysis Date = 07/15/16 Pct Recovery = 103% Analysis Date = 07/10/16 Pct Recovery = 103% Analysis Date = 07/10/16 Pct Recovery = 103% Analysis Date = 07/05/16 Pct Recovery = 104% Analysis Date = 07/05/16 Pct Recovery = 104% Analysis Date = 06/30/16 Pct Recovery = 104% Analysis Date = 06/30/16 Pct Recovery = 104% Analysis Date = 06/26/16 Pct Recovery = 105% Analysis Date = 06/26/16 Pct Recovery = 105% Analysis Date = 06/21/16 Pct Recovery = 105% Analysis Date = 06/21/16 Pct Recovery = 105% Analysis Date = 06/16/16 Pct Recovery = 105% Analysis Date = 06/16/16 Pct Recovery = 105% Analysis Date = 06/11/16 Pct Recovery = 106% Analysis Date = 06/11/16 Pct Recovery = 106% Analysis Date = 06/06/16 Pct Recovery = 106% Analysis Date = 06/06/16 Pct Recovery = 106% Analysis Date = 06/02/16 Pct Recovery = 107% Analysis Date = 06/02/16 Pct Recovery = 107% Analysis Date = 05/28/16 Pct Recovery = 107% Analysis Date = 05/28/16 Pct Recovery = 107% Analysis Date = 05/23/16 Pct Recovery = 107% Analysis Date = 05/23/16 Pct Recovery = 107% Analysis Date = 05/18/16 Pct Recovery = 108% Analysis Date = 05/18/16 Pct Recovery = 108% Analysis Date = 05/13/16 Pct Recovery = 108% Analysis Date = 05/13/16 Pct Recovery = 108% Analysis Date = 05/09/16 Pct Recovery = 109% Analysis Date = 05/09/16 Pct Recovery = 109% Analysis Date = 05/04/16 Pct Recovery = 109% Analysis Date = 05/04/16 Pct Recovery = 109% Analysis Date = 04/29/16 Pct Recovery = 110% Analysis Date = 04/29/16 Pct Recovery = 110% Analysis Date = 04/24/16 Pct Recovery = 110% Analysis Date = 04/24/16 Pct Recovery = 110% Analysis Date = 04/19/16 Pct Recovery = 110% Analysis Date = 04/19/16 Pct Recovery = 110% Analysis Date = 04/15/16 Pct Recovery = 111% Analysis Date = 04/15/16 Pct Recovery = 111% Analysis Date = 04/10/16 Pct Recovery = 111% Analysis Date = 04/10/16 Pct Recovery = 111% Analysis Date = 04/05/16 Pct Recovery = 111% Analysis Date = 04/05/16 Pct Recovery = 111% Analysis Date = 03/31/16 Pct Recovery = 112% Analysis Date = 03/31/16 Pct Recovery = 112% Analysis Date = 03/26/16 Pct Recovery = 112% Analysis Date = 03/26/16 Pct Recovery = 112% Analysis Date = 03/22/16 Pct Recovery = 112% Analysis Date = 03/22/16 Pct Recovery = 112% Analysis Date = 03/17/16 Pct Recovery = 113% Analysis Date = 03/17/16 Pct Recovery = 113% Analysis Date = 03/12/16 Pct Recovery = 113% Analysis Date = 03/12/16 Pct Recovery = 113% Analysis Date = 03/07/16 Pct Recovery = 114% Analysis Date = 03/07/16 Pct Recovery = 114% Analysis Date = 03/02/16 Pct Recovery = 114% Analysis Date = 03/02/16 Pct Recovery = 114% Analysis Date = 02/27/16 Pct Recovery = 114% Analysis Date = 02/27/16 Pct Recovery = 114% Analysis Date = 02/22/16 Pct Recovery = 115% Analysis Date = 02/22/16 Pct Recovery = 115% Analysis Date = 02/17/16 Pct Recovery = 115% Analysis Date = 02/17/16 Pct Recovery = 115% Analysis Date = 02/12/16 Pct Recovery = 115% Analysis Date = 02/12/16 Pct Recovery = 115% Analysis Date = 02/07/16 Pct Recovery = 116% Analysis Date = 02/07/16 Pct Recovery = 116% Analysis Date = 02/03/16 Pct Recovery = 116% Analysis Date = 02/03/16 Pct Recovery = 116% Analysis Date = 01/29/16 Pct Recovery = 116% Analysis Date = 01/29/16 Pct Recovery = 116% Analysis Date = 01/24/16 Pct Recovery = 116% Analysis Date = 01/24/16 Pct Recovery = 116% Analysis Date = 01/19/16 Pct Recovery = 116% Analysis Date = 01/19/16 Pct Recovery = 116% Analysis Date = 01/14/16 Pct Recovery = 116% Analysis Date = 01/14/16 Pct Recovery = 116% Analysis Date = 01/10/16 Pct Recovery = 116% Analysis Date = 01/10/16 Pct Recovery = 116% Analysis Date = 01/05/16 Pct Recovery = 116% Analysis Date = 01/05/16 Pct Recovery = 116% Analysis Date = 12/31/15 Pct Recovery = 117% Analysis Date = 12/31/15 Pct Recovery = 117% Analysis Date = 12/26/15 Pct Recovery = 117% Analysis Date = 12/26/15 Pct Recovery = 117% Analysis Date = 12/21/15 Pct Recovery = 117% Analysis Date = 12/21/15 Pct Recovery = 117% Analysis Date = 12/17/15 Pct Recovery = 117% Analysis Date = 12/17/15 Pct Recovery = 117% Analysis Date = 12/12/15 Pct Recovery = 117% Analysis Date = 12/12/15 Pct Recovery = 117% Analysis Date = 12/07/15 Pct Recovery = 117% Analysis Date = 12/07/15 Pct Recovery = 117% Analysis Date = 12/02/15 Pct Recovery = 117% Analysis Date = 12/02/15 Pct Recovery = 117% Analysis Date = 11/27/15 Pct Recovery = 117% Analysis Date = 11/27/15 Pct Recovery = 117% Analysis Date = 11/23/15 Pct Recovery = 117% Analysis Date = 11/23/15 Pct Recovery = 117% Analysis Date = 11/18/15 Pct Recovery = 117% Analysis Date = 11/18/15 Pct Recovery = 117% Analysis Date = 11/13/15 Pct Recovery = 117% Analysis Date = 11/13/15 Pct Recovery = 117% Analysis Date = 11/08/15 Pct Recovery = 117% Analysis Date = 11/08/15 Pct Recovery = 117% Analysis Date = 11/03/15 Pct Recovery = 116% Analysis Date = 11/03/15 Pct Recovery = 116% Analysis Date = 10/30/15 Pct Recovery = 116% Analysis Date = 10/30/15 Pct Recovery = 116% Analysis Date = 10/25/15 Pct Recovery = 116% Analysis Date = 10/25/15 Pct Recovery = 116% Analysis Date = 10/20/15 Pct Recovery = 116% Analysis Date = 10/20/15 Pct Recovery = 116% Analysis Date = 10/15/15 Pct Recovery = 115% Analysis Date = 10/15/15 Pct Recovery = 115% Analysis Date = 10/10/15 Pct Recovery = 115% Analysis Date = 10/10/15 Pct Recovery = 115% Analysis Date = 10/06/15 Pct Recovery = 115% Analysis Date = 10/06/15 Pct Recovery = 115% Analysis Date = 10/01/15 Pct Recovery = 114% Analysis Date = 10/01/15 Pct Recovery = 114% Analysis Date = 09/26/15 Pct Recovery = 114% Analysis Date = 09/26/15 Pct Recovery = 114% Analysis Date = 09/21/15 Pct Recovery = 113% Analysis Date = 09/21/15 Pct Recovery = 113% Analysis Date = 09/16/15 Pct Recovery = 113% Analysis Date = 09/16/15 Pct Recovery = 113% Analysis Date = 09/12/15 Pct Recovery = 113% Analysis Date = 09/12/15 Pct Recovery = 113% Analysis Date = 09/07/15 Pct Recovery = 112% Analysis Date = 09/07/15 Pct Recovery = 112% Analysis Date = 09/02/15 Pct Recovery = 112% Analysis Date = 09/02/15 Pct Recovery = 112% Analysis Date = 08/28/15 Pct Recovery = 112% Analysis Date = 08/28/15 Pct Recovery = 112% Analysis Date = 08/23/15 Pct Recovery = 111% Analysis Date = 08/23/15 Pct Recovery = 111% Analysis Date = 08/19/15 Pct Recovery = 111% Analysis Date = 08/19/15 Pct Recovery = 111% Analysis Date = 08/14/15 Pct Recovery = 110% Analysis Date = 08/14/15 Pct Recovery = 110% Analysis Date = 08/09/15 Pct Recovery = 110% Analysis Date = 08/09/15 Pct Recovery = 110% Analysis Date = 08/04/15 Pct Recovery = 110% Analysis Date = 08/04/15 Pct Recovery = 110% Analysis Date = 07/30/15 Pct Recovery = 109% Analysis Date = 07/30/15 Pct Recovery = 109% Analysis Date = 07/26/15 Pct Recovery = 109% Analysis Date = 07/26/15 Pct Recovery = 109% Analysis Date = 07/21/15 Pct Recovery = 109% Analysis Date = 07/21/15 Pct Recovery = 109% Analysis Date = 07/16/15 Pct Recovery = 108% Analysis Date = 07/16/15 Pct Recovery = 108% Analysis Date = 07/11/15 Pct Recovery = 108% Analysis Date = 07/11/15 Pct Recovery = 108% Analysis Date = 07/06/15 Pct Recovery = 108% Analysis Date = 07/06/15 Pct Recovery = 108% Analysis Date = 07/02/15 Pct Recovery = 107% Analysis Date = 07/02/15 Pct Recovery = 107% Analysis Date = 06/27/15 Pct Recovery = 107% Analysis Date = 06/27/15 Pct Recovery = 107% Analysis Date = 06/22/15 Pct Recovery = 107% Analysis Date = 06/22/15 Pct Recovery = 107% Analysis Date = 06/17/15 Pct Recovery = 106% Analysis Date = 06/17/15 Pct Recovery = 106% Analysis Date = 06/12/15 Pct Recovery = 106% Analysis Date = 06/12/15 Pct Recovery = 106% Analysis Date = 06/08/15 Pct Recovery = 106% Analysis Date = 06/08/15 Pct Recovery = 106% Analysis Date = 06/03/15 Pct Recovery = 106% Analysis Date = 06/03/15 Pct Recovery = 106% Analysis Date = 05/29/15 Pct Recovery = 106% Analysis Date = 05/29/15 Pct Recovery = 106% Analysis Date = 05/24/15 Pct Recovery = 106% Analysis Date = 05/24/15 Pct Recovery = 106% Analysis Date = 05/19/15 Pct Recovery = 106% Analysis Date = 05/19/15 Pct Recovery = 106% Analysis Date = 05/15/15 Pct Recovery = 106% Analysis Date = 05/15/15 Pct Recovery = 106% Analysis Date = 05/10/15 Pct Recovery = 106% Analysis Date = 05/10/15 Pct Recovery = 106% Analysis Date = 05/05/15 Pct Recovery = 106% Analysis Date = 05/05/15 Pct Recovery = 106% Analysis Date = 04/30/15 Pct Recovery = 106% Analysis Date = 04/30/15 Pct Recovery = 106% Analysis Date = 04/25/15 Pct Recovery = 106% Analysis Date = 04/25/15 Pct Recovery = 106% Analysis Date = 04/21/15 Pct Recovery = 106% Analysis Date = 04/21/15 Pct Recovery = 106% Analysis Date = 04/16/15 Pct Recovery = 106% Analysis Date = 04/16/15 Pct Recovery = 106% Analysis Date = 04/11/15 Pct Recovery = 106% Analysis Date = 04/11/15 Pct Recovery = 106% Analysis Date = 04/06/15 Pct Recovery = 105% Analysis Date = 04/06/15 Pct Recovery = 105% Analysis Date = 04/01/15 Pct Recovery = 105% Analysis Date = 04/01/15 Pct Recovery = 105% Analysis Date = 03/28/15 Pct Recovery = 105% Analysis Date = 03/28/15 Pct Recovery = 105% Analysis Date = 03/23/15 Pct Recovery = 105% Analysis Date = 03/23/15 Pct Recovery = 105% Analysis Date = 03/18/15 Pct Recovery = 105% Analysis Date = 03/18/15 Pct Recovery = 105% Analysis Date = 03/13/15 Pct Recovery = 105% Analysis Date = 03/13/15 Pct Recovery = 105% Analysis Date = 03/08/15 Pct Recovery = 105% Analysis Date = 03/08/15 Pct Recovery = 105% Analysis Date = 03/04/15 Pct Recovery = 105% Analysis Date = 03/04/15 Pct Recovery = 105% Analysis Date = 02/27/15 Pct Recovery = 106% Analysis Date = 02/27/15 Pct Recovery = 106% Analysis Date = 02/22/15 Pct Recovery = 106% Analysis Date = 02/22/15 Pct Recovery = 106% Analysis Date = 02/17/15 Pct Recovery = 106% Analysis Date = 02/17/15 Pct Recovery = 106% Analysis Date = 02/12/15 Pct Recovery = 106% Analysis Date = 02/12/15 Pct Recovery = 106% Analysis Date = 02/08/15 Pct Recovery = 107% Analysis Date = 02/08/15 Pct Recovery = 107% Analysis Date = 02/03/15 Pct Recovery = 107% Analysis Date = 02/03/15 Pct Recovery = 107% Analysis Date = 01/29/15 Pct Recovery = 107% Analysis Date = 01/29/15 Pct Recovery = 107% Analysis Date = 01/24/15 Pct Recovery = 108% Analysis Date = 01/24/15 Pct Recovery = 108% Analysis Date = 01/19/15 Pct Recovery = 108% Analysis Date = 01/19/15 Pct Recovery = 108% Analysis Date = 01/15/15 Pct Recovery = 108% Analysis Date = 01/15/15 Pct Recovery = 108% Analysis Date = 01/10/15 Pct Recovery = 109% Analysis Date = 01/10/15 Pct Recovery = 109% Analysis Date = 01/05/15 Pct Recovery = 109% Analysis Date = 01/05/15 Pct Recovery = 109% Analysis Date = 12/31/14 Pct Recovery = 109% Analysis Date = 12/31/14 Pct Recovery = 109% Analysis Date = 12/26/14 Pct Recovery = 110% Analysis Date = 12/26/14 Pct Recovery = 110% Analysis Date = 12/22/14 Pct Recovery = 110% Analysis Date = 12/22/14 Pct Recovery = 110% Analysis Date = 12/17/14 Pct Recovery = 110% Analysis Date = 12/17/14 Pct Recovery = 110% Analysis Date = 12/12/14 Pct Recovery = 110% Analysis Date = 12/12/14 Pct Recovery = 110% Analysis Date = 12/07/14 Pct Recovery = 111% Analysis Date = 12/07/14 Pct Recovery = 111% Analysis Date = 12/02/14 Pct Recovery = 111% Analysis Date = 12/02/14 Pct Recovery = 111% Analysis Date = 11/28/14 Pct Recovery = 111% Analysis Date = 11/28/14 Pct Recovery = 111% Analysis Date = 11/23/14 Pct Recovery = 112% Analysis Date = 11/23/14 Pct Recovery = 112% Analysis Date = 11/18/14 Pct Recovery = 112% Analysis Date = 11/18/14 Pct Recovery = 112% Analysis Date = 11/13/14 Pct Recovery = 112% Analysis Date = 11/13/14 Pct Recovery = 112% Analysis Date = 11/08/14 Pct Recovery = 113% Analysis Date = 11/08/14 Pct Recovery = 113% Analysis Date = 11/04/14 Pct Recovery = 113% Analysis Date = 11/04/14 Pct Recovery = 113% Analysis Date = 10/30/14 Pct Recovery = 113% Analysis Date = 10/30/14 Pct Recovery = 113% Analysis Date = 10/25/14 Pct Recovery = 114% Analysis Date = 10/25/14 Pct Recovery = 114% Analysis Date = 10/20/14 Pct Recovery = 114% Analysis Date = 10/20/14 Pct Recovery = 114% Analysis Date = 10/15/14 Pct Recovery = 115% Analysis Date = 10/15/14 Pct Recovery = 115% Analysis Date = 10/11/14 Pct Recovery = 115% Analysis Date = 10/11/14 Pct Recovery = 115% Analysis Date = 10/06/14 Pct Recovery = 116% Analysis Date = 10/06/14 Pct Recovery = 116% Analysis Date = 10/01/14 Pct Recovery = 116% Analysis Date = 10/01/14 Pct Recovery = 116% Analysis Date = 09/26/14 Pct Recovery = 116% Analysis Date = 09/26/14 Pct Recovery = 116% Analysis Date = 09/21/14 Pct Recovery = 117% Analysis Date = 09/21/14 Pct Recovery = 117% Analysis Date = 09/17/14 Pct Recovery = 117% Analysis Date = 09/17/14 Pct Recovery = 117% Analysis Date = 09/12/14 Pct Recovery = 118% Analysis Date = 09/12/14 Pct Recovery = 118% Analysis Date = 09/07/14 Pct Recovery = 118% Analysis Date = 09/07/14 Pct Recovery = 118% Analysis Date = 09/02/14 Pct Recovery = 118% Analysis Date = 09/02/14 Pct Recovery = 118% Analysis Date = 08/28/14 Pct Recovery = 119% Analysis Date = 08/28/14 Pct Recovery = 119% Analysis Date = 08/24/14 Pct Recovery = 119% Analysis Date = 08/24/14 Pct Recovery = 119% Analysis Date = 08/19/14 Pct Recovery = 120% Analysis Date = 08/19/14 Pct Recovery = 120% Analysis Date = 08/14/14 Pct Recovery = 120% Analysis Date = 08/14/14 Pct Recovery = 120% Analysis Date = 08/09/14 Pct Recovery = 121% Analysis Date = 08/09/14 Pct Recovery = 121% Analysis Date = 08/04/14 Pct Recovery = 121% Analysis Date = 08/04/14 Pct Recovery = 121% Analysis Date = 07/31/14 Pct Recovery = 122% Analysis Date = 07/31/14 Pct Recovery = 122% Analysis Date = 07/26/14 Pct Recovery = 122% Analysis Date = 07/26/14 Pct Recovery = 122% Analysis Date = 07/21/14 Pct Recovery = 123% Analysis Date = 07/21/14 Pct Recovery = 123% Analysis Date = 07/16/14 Pct Recovery = 123% Analysis Date = 07/16/14 Pct Recovery = 123% Analysis Date = 07/11/14 Pct Recovery = 124% Analysis Date = 07/11/14 Pct Recovery = 124% Analysis Date = 07/07/14 Pct Recovery = 124% Analysis Date = 07/07/14 Pct Recovery = 124% Analysis Date = 07/02/14 Pct Recovery = 125% Analysis Date = 07/02/14 Pct Recovery = 125% Analysis Date = 06/27/14 Pct Recovery = 125% Analysis Date = 06/27/14 Pct Recovery = 125% Analysis Date = 06/22/14 Pct Recovery = 126% Analysis Date = 06/22/14 Pct Recovery = 126% Analysis Date = 06/17/14 Pct Recovery = 126% Analysis Date = 06/17/14 Pct Recovery = 126% Analysis Date = 06/13/14 Pct Recovery = 127% Analysis Date = 06/13/14 Pct Recovery = 127% Analysis Date = 06/08/14 Pct Recovery = 127% Analysis Date = 06/08/14 Pct Recovery = 127% Analysis Date = 06/03/14 Pct Recovery = 128% Analysis Date = 06/03/14 Pct Recovery = 128% Analysis Date = 05/29/14 Pct Recovery = 128% Analysis Date = 05/29/14 Pct Recovery = 128% Analysis Date = 05/24/14 Pct Recovery = 129% Analysis Date = 05/24/14 Pct Recovery = 129% Analysis Date = 05/20/14 Pct Recovery = 130% Analysis Date = 05/20/14 Pct Recovery = 130% Analysis Date = 05/15/14 Pct Recovery = 130% Analysis Date = 05/15/14 Pct Recovery = 130% Analysis Date = 05/10/14 Pct Recovery = 131% Analysis Date = 05/10/14 Pct Recovery = 131% Analysis Date = 05/05/14 Pct Recovery = 131% Analysis Date = 05/05/14 Pct Recovery = 131% Analysis Date = 05/01/14 Pct Recovery = 132% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
CARBON DISULFIDE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 47 110% 21% 107% 19%
Total 47 110% 21% 107% 19%

Sample Statistics
CARBON DISULFIDE

Characteristic N % % Basis
Plotted 47 100% Spiked
Estimated Values 47 100% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 47 .  
False Negatives 0 0% 0 out of 47
Not Spiked 25 .  
False Positives 2 8% 2 out of 25

BQS OBSP Determination:
CHLOROBENZENE
METHOD: 4440 , TESTIDCODE: 34301GCM66
Open Data Set

Analysis Date = 12/16/16 SpikeMix = NSI 041816AVOC: 40 µl & ChemService 5082900: 40 µl Pct Recovery = 111% Analysis Date = 08/04/16 SpikeMix = Crescent 03FF058: 40 µl & Supelco LC20141V: 40 µl Pct Recovery = 95% Analysis Date = 07/20/16 SpikeMix = Supelco LC20141V: 40 µl & Accu 216041125: 40 µl Pct Recovery = 91% Analysis Date = 11/21/16 SpikeMix = Crescent 03FF058: 25 µl & Supelco LC20141V: 25 µl Pct Recovery = 93% Analysis Date = 09/08/16 SpikeMix = Supelco LC20141V: 25 µl & Accu 216041125: 25 µl Pct Recovery = 93% Analysis Date = 08/26/16 SpikeMix = NSI 041816AVOC: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 112% Analysis Date = 08/12/16 SpikeMix = ChemService 5082900: 25 µl & Phenova B20160319: 25 µl Pct Recovery = 101% Analysis Date = 06/30/16 SpikeMix = Crescent 03FF058: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 98% Analysis Date = 04/09/15 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 94% Analysis Date = 03/06/15 SpikeMix = ERA 0227-14-06.1A: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 100% Analysis Date = 11/14/14 SpikeMix = Crescent 03DD004: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 93% Analysis Date = 08/16/14 SpikeMix = ERA 0227-14-06.1A: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 93% Analysis Date = 07/01/14 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 102% Analysis Date = 11/22/14 SpikeMix = NSI 032614: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 96% Analysis Date = 06/10/14 SpikeMix = Crescent 03DD004: 20 µl & NSI 032614: 20 µl Pct Recovery = 98% Analysis Date = 06/10/14 SpikeMix = NSI 032614: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 98% Analysis Date = 05/01/14 SpikeMix = Accu 214031115: 20 µl & NSI 032614: 20 µl Pct Recovery = 92% Analysis Date = 09/29/15 SpikeMix = Accu 215041380: 25 µl & ERA 0406-15-03: 25 µl Pct Recovery = 99% Analysis Date = 06/16/15 SpikeMix = ERA 0406-15-03: 25 µl & Supelco LC13545: 25 µl Pct Recovery = 89% Analysis Date = 07/13/15 SpikeMix = Crescent 04EE008: 25 µl & NSI 050515AVOC: 25 µl Pct Recovery = 93% Analysis Date = 11/29/16 SpikeMix = ChemService 5082900: 15 µl & Phenova B20160319: 15 µl Pct Recovery = 95% Analysis Date = 10/13/16 SpikeMix = NSI 041816AVOC: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 104% Analysis Date = 09/28/16 SpikeMix = Crescent 03FF058: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 114% Analysis Date = 06/30/16 SpikeMix = ChemService 5082900: 15 µl & Accu 216041125: 15 µl Pct Recovery = 99% Analysis Date = 06/10/16 SpikeMix = NSI 041816AVOC: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 118% Analysis Date = 05/27/16 SpikeMix = Phenova B20160319: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 100% Analysis Date = 04/26/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 102% Analysis Date = 03/04/16 SpikeMix = Accu 215041380: 15 µl & ERA 0406-15-03: 15 µl Pct Recovery = 97% Analysis Date = 02/05/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 97% Analysis Date = 10/16/15 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 103% Analysis Date = 11/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 91% Analysis Date = 10/17/15 SpikeMix = Crescent 04EE008: 15 µl & NSI 050515AVOC: 15 µl Pct Recovery = 91% Analysis Date = 06/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Accu 215041380: 15 µl Pct Recovery = 97% Analysis Date = 01/13/15 SpikeMix = Accu 214031115: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 94% Analysis Date = 10/21/14 SpikeMix = ERA 0227-14-06.1A: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 99% Analysis Date = 10/04/14 SpikeMix = Crescent 03DD004: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 98% Analysis Date = 07/11/14 SpikeMix = Spex Organics C1140417015: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 99% Analysis Date = 09/09/14 SpikeMix = Accu 214031115: 10 µl & NSI 032614: 10 µl Pct Recovery = 111% Analysis Date = 09/09/14 SpikeMix = NSI 032614: 10 µl & Spex Organics C1140417015: 10 µl Pct Recovery = 117% Analysis Date = 07/29/14 SpikeMix = Crescent 03DD004: 10 µl & NSI 032614: 10 µl Pct Recovery = 102% Analysis Date = 05/30/14 SpikeMix = NSI 032614: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 88% Analysis Date = 11/20/15 SpikeMix = Accu 215041380: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 105% Analysis Date = 07/31/15 SpikeMix = Crescent 04EE008: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 95% Analysis Date = 06/27/15 SpikeMix = ERA 0406-15-03: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 106% Analysis Date = 03/17/16 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 97% Analysis Date = 01/27/16 SpikeMix = Crescent 04EE008: 10 µl & NSI 050515AVOC: 10 µl Pct Recovery = 98% Analysis Date = 12/10/15 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 100% Analysis Date = 09/03/15 SpikeMix = NSI 050515AVOC: 10 µl & Spex Organics EN150428007: 10 µl Pct Recovery = 94% Analysis Date = 12/15/16 Pct Recovery = 103% Analysis Date = 12/11/16 Pct Recovery = 103% Analysis Date = 12/11/16 Pct Recovery = 103% Analysis Date = 12/06/16 Pct Recovery = 103% Analysis Date = 12/06/16 Pct Recovery = 103% Analysis Date = 12/01/16 Pct Recovery = 102% Analysis Date = 12/01/16 Pct Recovery = 102% Analysis Date = 11/26/16 Pct Recovery = 102% Analysis Date = 11/26/16 Pct Recovery = 102% Analysis Date = 11/21/16 Pct Recovery = 102% Analysis Date = 11/21/16 Pct Recovery = 102% Analysis Date = 11/17/16 Pct Recovery = 102% Analysis Date = 11/17/16 Pct Recovery = 102% Analysis Date = 11/12/16 Pct Recovery = 102% Analysis Date = 11/12/16 Pct Recovery = 102% Analysis Date = 11/07/16 Pct Recovery = 102% Analysis Date = 11/07/16 Pct Recovery = 102% Analysis Date = 11/02/16 Pct Recovery = 102% Analysis Date = 11/02/16 Pct Recovery = 102% Analysis Date = 10/28/16 Pct Recovery = 102% Analysis Date = 10/28/16 Pct Recovery = 102% Analysis Date = 10/24/16 Pct Recovery = 102% Analysis Date = 10/24/16 Pct Recovery = 102% Analysis Date = 10/19/16 Pct Recovery = 102% Analysis Date = 10/19/16 Pct Recovery = 102% Analysis Date = 10/14/16 Pct Recovery = 102% Analysis Date = 10/14/16 Pct Recovery = 102% Analysis Date = 10/09/16 Pct Recovery = 102% Analysis Date = 10/09/16 Pct Recovery = 102% Analysis Date = 10/04/16 Pct Recovery = 102% Analysis Date = 10/04/16 Pct Recovery = 102% Analysis Date = 09/30/16 Pct Recovery = 102% Analysis Date = 09/30/16 Pct Recovery = 102% Analysis Date = 09/25/16 Pct Recovery = 102% Analysis Date = 09/25/16 Pct Recovery = 102% Analysis Date = 09/20/16 Pct Recovery = 102% Analysis Date = 09/20/16 Pct Recovery = 102% Analysis Date = 09/15/16 Pct Recovery = 102% Analysis Date = 09/15/16 Pct Recovery = 102% Analysis Date = 09/10/16 Pct Recovery = 102% Analysis Date = 09/10/16 Pct Recovery = 102% Analysis Date = 09/06/16 Pct Recovery = 102% Analysis Date = 09/06/16 Pct Recovery = 102% Analysis Date = 09/01/16 Pct Recovery = 101% Analysis Date = 09/01/16 Pct Recovery = 101% Analysis Date = 08/27/16 Pct Recovery = 101% Analysis Date = 08/27/16 Pct Recovery = 101% Analysis Date = 08/22/16 Pct Recovery = 101% Analysis Date = 08/22/16 Pct Recovery = 101% Analysis Date = 08/17/16 Pct Recovery = 101% Analysis Date = 08/17/16 Pct Recovery = 101% Analysis Date = 08/13/16 Pct Recovery = 101% Analysis Date = 08/13/16 Pct Recovery = 101% Analysis Date = 08/08/16 Pct Recovery = 101% Analysis Date = 08/08/16 Pct Recovery = 101% Analysis Date = 08/03/16 Pct Recovery = 101% Analysis Date = 08/03/16 Pct Recovery = 101% Analysis Date = 07/29/16 Pct Recovery = 101% Analysis Date = 07/29/16 Pct Recovery = 101% Analysis Date = 07/24/16 Pct Recovery = 101% Analysis Date = 07/24/16 Pct Recovery = 101% Analysis Date = 07/20/16 Pct Recovery = 101% Analysis Date = 07/20/16 Pct Recovery = 101% Analysis Date = 07/15/16 Pct Recovery = 101% Analysis Date = 07/15/16 Pct Recovery = 101% Analysis Date = 07/10/16 Pct Recovery = 101% Analysis Date = 07/10/16 Pct Recovery = 101% Analysis Date = 07/05/16 Pct Recovery = 101% Analysis Date = 07/05/16 Pct Recovery = 101% Analysis Date = 06/30/16 Pct Recovery = 101% Analysis Date = 06/30/16 Pct Recovery = 101% Analysis Date = 06/26/16 Pct Recovery = 101% Analysis Date = 06/26/16 Pct Recovery = 101% Analysis Date = 06/21/16 Pct Recovery = 101% Analysis Date = 06/21/16 Pct Recovery = 101% Analysis Date = 06/16/16 Pct Recovery = 101% Analysis Date = 06/16/16 Pct Recovery = 101% Analysis Date = 06/11/16 Pct Recovery = 101% Analysis Date = 06/11/16 Pct Recovery = 101% Analysis Date = 06/06/16 Pct Recovery = 101% Analysis Date = 06/06/16 Pct Recovery = 101% Analysis Date = 06/02/16 Pct Recovery = 100% Analysis Date = 06/02/16 Pct Recovery = 100% Analysis Date = 05/28/16 Pct Recovery = 100% Analysis Date = 05/28/16 Pct Recovery = 100% Analysis Date = 05/23/16 Pct Recovery = 100% Analysis Date = 05/23/16 Pct Recovery = 100% Analysis Date = 05/18/16 Pct Recovery = 100% Analysis Date = 05/18/16 Pct Recovery = 100% Analysis Date = 05/13/16 Pct Recovery = 100% Analysis Date = 05/13/16 Pct Recovery = 100% Analysis Date = 05/09/16 Pct Recovery = 100% Analysis Date = 05/09/16 Pct Recovery = 100% Analysis Date = 05/04/16 Pct Recovery = 100% Analysis Date = 05/04/16 Pct Recovery = 100% Analysis Date = 04/29/16 Pct Recovery = 100% Analysis Date = 04/29/16 Pct Recovery = 100% Analysis Date = 04/24/16 Pct Recovery = 100% Analysis Date = 04/24/16 Pct Recovery = 100% Analysis Date = 04/19/16 Pct Recovery = 100% Analysis Date = 04/19/16 Pct Recovery = 100% Analysis Date = 04/15/16 Pct Recovery = 100% Analysis Date = 04/15/16 Pct Recovery = 100% Analysis Date = 04/10/16 Pct Recovery = 100% Analysis Date = 04/10/16 Pct Recovery = 100% Analysis Date = 04/05/16 Pct Recovery = 100% Analysis Date = 04/05/16 Pct Recovery = 100% Analysis Date = 03/31/16 Pct Recovery = 100% Analysis Date = 03/31/16 Pct Recovery = 100% Analysis Date = 03/26/16 Pct Recovery = 100% Analysis Date = 03/26/16 Pct Recovery = 100% Analysis Date = 03/22/16 Pct Recovery = 100% Analysis Date = 03/22/16 Pct Recovery = 100% Analysis Date = 03/17/16 Pct Recovery = 100% Analysis Date = 03/17/16 Pct Recovery = 100% Analysis Date = 03/12/16 Pct Recovery = 99% Analysis Date = 03/12/16 Pct Recovery = 99% Analysis Date = 03/07/16 Pct Recovery = 99% Analysis Date = 03/07/16 Pct Recovery = 99% Analysis Date = 03/02/16 Pct Recovery = 99% Analysis Date = 03/02/16 Pct Recovery = 99% Analysis Date = 02/27/16 Pct Recovery = 99% Analysis Date = 02/27/16 Pct Recovery = 99% Analysis Date = 02/22/16 Pct Recovery = 99% Analysis Date = 02/22/16 Pct Recovery = 99% Analysis Date = 02/17/16 Pct Recovery = 99% Analysis Date = 02/17/16 Pct Recovery = 99% Analysis Date = 02/12/16 Pct Recovery = 99% Analysis Date = 02/12/16 Pct Recovery = 99% Analysis Date = 02/07/16 Pct Recovery = 99% Analysis Date = 02/07/16 Pct Recovery = 99% Analysis Date = 02/03/16 Pct Recovery = 99% Analysis Date = 02/03/16 Pct Recovery = 99% Analysis Date = 01/29/16 Pct Recovery = 99% Analysis Date = 01/29/16 Pct Recovery = 99% Analysis Date = 01/24/16 Pct Recovery = 99% Analysis Date = 01/24/16 Pct Recovery = 99% Analysis Date = 01/19/16 Pct Recovery = 99% Analysis Date = 01/19/16 Pct Recovery = 99% Analysis Date = 01/14/16 Pct Recovery = 99% Analysis Date = 01/14/16 Pct Recovery = 99% Analysis Date = 01/10/16 Pct Recovery = 99% Analysis Date = 01/10/16 Pct Recovery = 99% Analysis Date = 01/05/16 Pct Recovery = 98% Analysis Date = 01/05/16 Pct Recovery = 98% Analysis Date = 12/31/15 Pct Recovery = 98% Analysis Date = 12/31/15 Pct Recovery = 98% Analysis Date = 12/26/15 Pct Recovery = 98% Analysis Date = 12/26/15 Pct Recovery = 98% Analysis Date = 12/21/15 Pct Recovery = 98% Analysis Date = 12/21/15 Pct Recovery = 98% Analysis Date = 12/17/15 Pct Recovery = 98% Analysis Date = 12/17/15 Pct Recovery = 98% Analysis Date = 12/12/15 Pct Recovery = 98% Analysis Date = 12/12/15 Pct Recovery = 98% Analysis Date = 12/07/15 Pct Recovery = 98% Analysis Date = 12/07/15 Pct Recovery = 98% Analysis Date = 12/02/15 Pct Recovery = 98% Analysis Date = 12/02/15 Pct Recovery = 98% Analysis Date = 11/27/15 Pct Recovery = 98% Analysis Date = 11/27/15 Pct Recovery = 98% Analysis Date = 11/23/15 Pct Recovery = 98% Analysis Date = 11/23/15 Pct Recovery = 98% Analysis Date = 11/18/15 Pct Recovery = 98% Analysis Date = 11/18/15 Pct Recovery = 98% Analysis Date = 11/13/15 Pct Recovery = 98% Analysis Date = 11/13/15 Pct Recovery = 98% Analysis Date = 11/08/15 Pct Recovery = 98% Analysis Date = 11/08/15 Pct Recovery = 98% Analysis Date = 11/03/15 Pct Recovery = 98% Analysis Date = 11/03/15 Pct Recovery = 98% Analysis Date = 10/30/15 Pct Recovery = 97% Analysis Date = 10/30/15 Pct Recovery = 97% Analysis Date = 10/25/15 Pct Recovery = 97% Analysis Date = 10/25/15 Pct Recovery = 97% Analysis Date = 10/20/15 Pct Recovery = 97% Analysis Date = 10/20/15 Pct Recovery = 97% Analysis Date = 10/15/15 Pct Recovery = 97% Analysis Date = 10/15/15 Pct Recovery = 97% Analysis Date = 10/10/15 Pct Recovery = 97% Analysis Date = 10/10/15 Pct Recovery = 97% Analysis Date = 10/06/15 Pct Recovery = 97% Analysis Date = 10/06/15 Pct Recovery = 97% Analysis Date = 10/01/15 Pct Recovery = 97% Analysis Date = 10/01/15 Pct Recovery = 97% Analysis Date = 09/26/15 Pct Recovery = 97% Analysis Date = 09/26/15 Pct Recovery = 97% Analysis Date = 09/21/15 Pct Recovery = 97% Analysis Date = 09/21/15 Pct Recovery = 97% Analysis Date = 09/16/15 Pct Recovery = 97% Analysis Date = 09/16/15 Pct Recovery = 97% Analysis Date = 09/12/15 Pct Recovery = 97% Analysis Date = 09/12/15 Pct Recovery = 97% Analysis Date = 09/07/15 Pct Recovery = 97% Analysis Date = 09/07/15 Pct Recovery = 97% Analysis Date = 09/02/15 Pct Recovery = 97% Analysis Date = 09/02/15 Pct Recovery = 97% Analysis Date = 08/28/15 Pct Recovery = 97% Analysis Date = 08/28/15 Pct Recovery = 97% Analysis Date = 08/23/15 Pct Recovery = 97% Analysis Date = 08/23/15 Pct Recovery = 97% Analysis Date = 08/19/15 Pct Recovery = 97% Analysis Date = 08/19/15 Pct Recovery = 97% Analysis Date = 08/14/15 Pct Recovery = 97% Analysis Date = 08/14/15 Pct Recovery = 97% Analysis Date = 08/09/15 Pct Recovery = 97% Analysis Date = 08/09/15 Pct Recovery = 97% Analysis Date = 08/04/15 Pct Recovery = 97% Analysis Date = 08/04/15 Pct Recovery = 97% Analysis Date = 07/30/15 Pct Recovery = 97% Analysis Date = 07/30/15 Pct Recovery = 97% Analysis Date = 07/26/15 Pct Recovery = 97% Analysis Date = 07/26/15 Pct Recovery = 97% Analysis Date = 07/21/15 Pct Recovery = 97% Analysis Date = 07/21/15 Pct Recovery = 97% Analysis Date = 07/16/15 Pct Recovery = 97% Analysis Date = 07/16/15 Pct Recovery = 97% Analysis Date = 07/11/15 Pct Recovery = 97% Analysis Date = 07/11/15 Pct Recovery = 97% Analysis Date = 07/06/15 Pct Recovery = 97% Analysis Date = 07/06/15 Pct Recovery = 97% Analysis Date = 07/02/15 Pct Recovery = 97% Analysis Date = 07/02/15 Pct Recovery = 97% Analysis Date = 06/27/15 Pct Recovery = 97% Analysis Date = 06/27/15 Pct Recovery = 97% Analysis Date = 06/22/15 Pct Recovery = 97% Analysis Date = 06/22/15 Pct Recovery = 97% Analysis Date = 06/17/15 Pct Recovery = 97% Analysis Date = 06/17/15 Pct Recovery = 97% Analysis Date = 06/12/15 Pct Recovery = 97% Analysis Date = 06/12/15 Pct Recovery = 97% Analysis Date = 06/08/15 Pct Recovery = 97% Analysis Date = 06/08/15 Pct Recovery = 97% Analysis Date = 06/03/15 Pct Recovery = 97% Analysis Date = 06/03/15 Pct Recovery = 97% Analysis Date = 05/29/15 Pct Recovery = 97% Analysis Date = 05/29/15 Pct Recovery = 97% Analysis Date = 05/24/15 Pct Recovery = 97% Analysis Date = 05/24/15 Pct Recovery = 97% Analysis Date = 05/19/15 Pct Recovery = 97% Analysis Date = 05/19/15 Pct Recovery = 97% Analysis Date = 05/15/15 Pct Recovery = 97% Analysis Date = 05/15/15 Pct Recovery = 97% Analysis Date = 05/10/15 Pct Recovery = 97% Analysis Date = 05/10/15 Pct Recovery = 97% Analysis Date = 05/05/15 Pct Recovery = 97% Analysis Date = 05/05/15 Pct Recovery = 97% Analysis Date = 04/30/15 Pct Recovery = 97% Analysis Date = 04/30/15 Pct Recovery = 97% Analysis Date = 04/25/15 Pct Recovery = 97% Analysis Date = 04/25/15 Pct Recovery = 97% Analysis Date = 04/21/15 Pct Recovery = 97% Analysis Date = 04/21/15 Pct Recovery = 97% Analysis Date = 04/16/15 Pct Recovery = 97% Analysis Date = 04/16/15 Pct Recovery = 97% Analysis Date = 04/11/15 Pct Recovery = 97% Analysis Date = 04/11/15 Pct Recovery = 97% Analysis Date = 04/06/15 Pct Recovery = 97% Analysis Date = 04/06/15 Pct Recovery = 97% Analysis Date = 04/01/15 Pct Recovery = 97% Analysis Date = 04/01/15 Pct Recovery = 97% Analysis Date = 03/28/15 Pct Recovery = 97% Analysis Date = 03/28/15 Pct Recovery = 97% Analysis Date = 03/23/15 Pct Recovery = 97% Analysis Date = 03/23/15 Pct Recovery = 97% Analysis Date = 03/18/15 Pct Recovery = 97% Analysis Date = 03/18/15 Pct Recovery = 97% Analysis Date = 03/13/15 Pct Recovery = 97% Analysis Date = 03/13/15 Pct Recovery = 97% Analysis Date = 03/08/15 Pct Recovery = 98% Analysis Date = 03/08/15 Pct Recovery = 98% Analysis Date = 03/04/15 Pct Recovery = 98% Analysis Date = 03/04/15 Pct Recovery = 98% Analysis Date = 02/27/15 Pct Recovery = 98% Analysis Date = 02/27/15 Pct Recovery = 98% Analysis Date = 02/22/15 Pct Recovery = 98% Analysis Date = 02/22/15 Pct Recovery = 98% Analysis Date = 02/17/15 Pct Recovery = 98% Analysis Date = 02/17/15 Pct Recovery = 98% Analysis Date = 02/12/15 Pct Recovery = 98% Analysis Date = 02/12/15 Pct Recovery = 98% Analysis Date = 02/08/15 Pct Recovery = 98% Analysis Date = 02/08/15 Pct Recovery = 98% Analysis Date = 02/03/15 Pct Recovery = 98% Analysis Date = 02/03/15 Pct Recovery = 98% Analysis Date = 01/29/15 Pct Recovery = 98% Analysis Date = 01/29/15 Pct Recovery = 98% Analysis Date = 01/24/15 Pct Recovery = 98% Analysis Date = 01/24/15 Pct Recovery = 98% Analysis Date = 01/19/15 Pct Recovery = 98% Analysis Date = 01/19/15 Pct Recovery = 98% Analysis Date = 01/15/15 Pct Recovery = 98% Analysis Date = 01/15/15 Pct Recovery = 98% Analysis Date = 01/10/15 Pct Recovery = 98% Analysis Date = 01/10/15 Pct Recovery = 98% Analysis Date = 01/05/15 Pct Recovery = 98% Analysis Date = 01/05/15 Pct Recovery = 98% Analysis Date = 12/31/14 Pct Recovery = 98% Analysis Date = 12/31/14 Pct Recovery = 98% Analysis Date = 12/26/14 Pct Recovery = 98% Analysis Date = 12/26/14 Pct Recovery = 98% Analysis Date = 12/22/14 Pct Recovery = 98% Analysis Date = 12/22/14 Pct Recovery = 98% Analysis Date = 12/17/14 Pct Recovery = 98% Analysis Date = 12/17/14 Pct Recovery = 98% Analysis Date = 12/12/14 Pct Recovery = 98% Analysis Date = 12/12/14 Pct Recovery = 98% Analysis Date = 12/07/14 Pct Recovery = 98% Analysis Date = 12/07/14 Pct Recovery = 98% Analysis Date = 12/02/14 Pct Recovery = 98% Analysis Date = 12/02/14 Pct Recovery = 98% Analysis Date = 11/28/14 Pct Recovery = 98% Analysis Date = 11/28/14 Pct Recovery = 98% Analysis Date = 11/23/14 Pct Recovery = 98% Analysis Date = 11/23/14 Pct Recovery = 98% Analysis Date = 11/18/14 Pct Recovery = 98% Analysis Date = 11/18/14 Pct Recovery = 98% Analysis Date = 11/13/14 Pct Recovery = 98% Analysis Date = 11/13/14 Pct Recovery = 98% Analysis Date = 11/08/14 Pct Recovery = 98% Analysis Date = 11/08/14 Pct Recovery = 98% Analysis Date = 11/04/14 Pct Recovery = 98% Analysis Date = 11/04/14 Pct Recovery = 98% Analysis Date = 10/30/14 Pct Recovery = 98% Analysis Date = 10/30/14 Pct Recovery = 98% Analysis Date = 10/25/14 Pct Recovery = 98% Analysis Date = 10/25/14 Pct Recovery = 98% Analysis Date = 10/20/14 Pct Recovery = 98% Analysis Date = 10/20/14 Pct Recovery = 98% Analysis Date = 10/15/14 Pct Recovery = 98% Analysis Date = 10/15/14 Pct Recovery = 98% Analysis Date = 10/11/14 Pct Recovery = 98% Analysis Date = 10/11/14 Pct Recovery = 98% Analysis Date = 10/06/14 Pct Recovery = 98% Analysis Date = 10/06/14 Pct Recovery = 98% Analysis Date = 10/01/14 Pct Recovery = 98% Analysis Date = 10/01/14 Pct Recovery = 98% Analysis Date = 09/26/14 Pct Recovery = 98% Analysis Date = 09/26/14 Pct Recovery = 98% Analysis Date = 09/21/14 Pct Recovery = 98% Analysis Date = 09/21/14 Pct Recovery = 98% Analysis Date = 09/17/14 Pct Recovery = 98% Analysis Date = 09/17/14 Pct Recovery = 98% Analysis Date = 09/12/14 Pct Recovery = 98% Analysis Date = 09/12/14 Pct Recovery = 98% Analysis Date = 09/07/14 Pct Recovery = 98% Analysis Date = 09/07/14 Pct Recovery = 98% Analysis Date = 09/02/14 Pct Recovery = 98% Analysis Date = 09/02/14 Pct Recovery = 98% Analysis Date = 08/28/14 Pct Recovery = 99% Analysis Date = 08/28/14 Pct Recovery = 99% Analysis Date = 08/24/14 Pct Recovery = 99% Analysis Date = 08/24/14 Pct Recovery = 99% Analysis Date = 08/19/14 Pct Recovery = 99% Analysis Date = 08/19/14 Pct Recovery = 99% Analysis Date = 08/14/14 Pct Recovery = 99% Analysis Date = 08/14/14 Pct Recovery = 99% Analysis Date = 08/09/14 Pct Recovery = 99% Analysis Date = 08/09/14 Pct Recovery = 99% Analysis Date = 08/04/14 Pct Recovery = 99% Analysis Date = 08/04/14 Pct Recovery = 99% Analysis Date = 07/31/14 Pct Recovery = 99% Analysis Date = 07/31/14 Pct Recovery = 99% Analysis Date = 07/26/14 Pct Recovery = 99% Analysis Date = 07/26/14 Pct Recovery = 99% Analysis Date = 07/21/14 Pct Recovery = 99% Analysis Date = 07/21/14 Pct Recovery = 99% Analysis Date = 07/16/14 Pct Recovery = 99% Analysis Date = 07/16/14 Pct Recovery = 99% Analysis Date = 07/11/14 Pct Recovery = 99% Analysis Date = 07/11/14 Pct Recovery = 99% Analysis Date = 07/07/14 Pct Recovery = 99% Analysis Date = 07/07/14 Pct Recovery = 99% Analysis Date = 07/02/14 Pct Recovery = 99% Analysis Date = 07/02/14 Pct Recovery = 99% Analysis Date = 06/27/14 Pct Recovery = 99% Analysis Date = 06/27/14 Pct Recovery = 99% Analysis Date = 06/22/14 Pct Recovery = 99% Analysis Date = 06/22/14 Pct Recovery = 99% Analysis Date = 06/17/14 Pct Recovery = 99% Analysis Date = 06/17/14 Pct Recovery = 99% Analysis Date = 06/13/14 Pct Recovery = 99% Analysis Date = 06/13/14 Pct Recovery = 99% Analysis Date = 06/08/14 Pct Recovery = 99% Analysis Date = 06/08/14 Pct Recovery = 99% Analysis Date = 06/03/14 Pct Recovery = 99% Analysis Date = 06/03/14 Pct Recovery = 99% Analysis Date = 05/29/14 Pct Recovery = 99% Analysis Date = 05/29/14 Pct Recovery = 99% Analysis Date = 05/24/14 Pct Recovery = 99% Analysis Date = 05/24/14 Pct Recovery = 99% Analysis Date = 05/20/14 Pct Recovery = 99% Analysis Date = 05/20/14 Pct Recovery = 99% Analysis Date = 05/15/14 Pct Recovery = 99% Analysis Date = 05/15/14 Pct Recovery = 99% Analysis Date = 05/10/14 Pct Recovery = 99% Analysis Date = 05/10/14 Pct Recovery = 99% Analysis Date = 05/05/14 Pct Recovery = 99% Analysis Date = 05/05/14 Pct Recovery = 99% Analysis Date = 05/01/14 Pct Recovery = 99% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
CHLOROBENZENE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 48 99% 7% 98% 6%
Total 48 99% 7% 98% 6%

Sample Statistics
CHLOROBENZENE

Characteristic N % % Basis
Plotted 48 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 48 .  
False Negatives 0 0% 0 out of 48
Not Spiked 25 .  
False Positives 1 4% 1 out of 25

BQS OBSP Determination:
CHLORODIFLUOROMETHANE
METHOD: 4440 , TESTIDCODE: 45028GCM66
Open Data Set

Analysis Date = 12/12/16 SpikeMix = Accu 216041125: 40 µl & Crescent 03FF058: 40 µl Pct Recovery = 68% Analysis Date = 07/20/16 SpikeMix = Supelco LC20141V: 40 µl & Accu 216041125: 40 µl Pct Recovery = 98% Analysis Date = 07/14/16 SpikeMix = Accu 216041125: 40 µl & NSI 041816AVOC: 40 µl Pct Recovery = 79% Analysis Date = 09/08/16 SpikeMix = Supelco LC20141V: 25 µl & Accu 216041125: 25 µl Pct Recovery = 79% Analysis Date = 05/24/16 SpikeMix = Accu 216041125: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 87% Analysis Date = 08/15/15 SpikeMix = Supelco LC13545: 25 µl & Crescent 04EE008: 25 µl Pct Recovery = 103% Analysis Date = 06/16/15 SpikeMix = ERA 0406-15-03: 25 µl & Supelco LC13545: 25 µl Pct Recovery = 94% Analysis Date = 10/13/16 SpikeMix = Accu 216041125: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 89% Analysis Date = 08/20/16 SpikeMix = Accu 216041125: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 89% Analysis Date = 06/30/16 SpikeMix = ChemService 5082900: 15 µl & Accu 216041125: 15 µl Pct Recovery = 61% Analysis Date = 04/26/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 101% Analysis Date = 04/02/16 SpikeMix = Supelco LC13545: 15 µl & Accu 215041380: 15 µl Pct Recovery = 111% Analysis Date = 02/05/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 115% Analysis Date = 12/18/15 SpikeMix = Supelco LC13545: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 96% Analysis Date = 11/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 106% Analysis Date = 10/16/15 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 102% Analysis Date = 05/09/15 SpikeMix = Spex Organics EN150428007: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 133% Analysis Date = 05/13/16 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 87% Analysis Date = 03/17/16 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 90% Analysis Date = 02/18/16 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 110% Analysis Date = 12/10/15 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 93% Analysis Date = 11/12/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 120% Analysis Date = 09/03/15 SpikeMix = NSI 050515AVOC: 10 µl & Spex Organics EN150428007: 10 µl Pct Recovery = 105% Analysis Date = 06/27/15 SpikeMix = ERA 0406-15-03: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 109% Analysis Date = 05/21/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 111% Analysis Date = 05/09/15 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 119% Analysis Date = 08/19/14 SpikeMix = Spex Organics C1140417015: 20 µl & Accu 214031115: 20 µl Pct Recovery = 111% Analysis Date = 07/01/14 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 108% Analysis Date = 05/01/14 SpikeMix = Accu 214031115: 20 µl & NSI 032614: 20 µl Pct Recovery = 124% Analysis Date = 06/10/14 SpikeMix = Crescent 03DD004: 20 µl & NSI 032614: 20 µl Pct Recovery = 72% Analysis Date = 09/09/14 SpikeMix = Accu 214031115: 10 µl & NSI 032614: 10 µl Pct Recovery = 135% Analysis Date = 07/23/14 SpikeMix = Spex Organics C1140417015: 10 µl & Accu 214031115: 10 µl Pct Recovery = 141% Analysis Date = 06/18/14 SpikeMix = Supelco LC06438: 10 µl & Accu 214031115: 10 µl Pct Recovery = 123% Analysis Date = 07/29/14 SpikeMix = Crescent 03DD004: 10 µl & NSI 032614: 10 µl Pct Recovery = 111% Analysis Date = 05/03/14 SpikeMix = Crescent 03DD004: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 126% Analysis Date = 04/09/15 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 106% Analysis Date = 03/19/15 SpikeMix = Spex Organics C1140417015: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 105% Analysis Date = 12/17/14 SpikeMix = Supelco LC06438: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 87% Analysis Date = 11/14/14 SpikeMix = Crescent 03DD004: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 69% Analysis Date = 01/13/15 SpikeMix = Accu 214031115: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 100% Analysis Date = 11/06/14 SpikeMix = Spex Organics C1140417015: 10 µl & Crescent 03DD004: 10 µl Pct Recovery = 87% Analysis Date = 10/04/14 SpikeMix = Crescent 03DD004: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 92% Analysis Date = 12/11/16 Pct Recovery = 73% Analysis Date = 12/07/16 Pct Recovery = 73% Analysis Date = 12/07/16 Pct Recovery = 73% Analysis Date = 12/02/16 Pct Recovery = 74% Analysis Date = 12/02/16 Pct Recovery = 74% Analysis Date = 11/27/16 Pct Recovery = 74% Analysis Date = 11/27/16 Pct Recovery = 74% Analysis Date = 11/22/16 Pct Recovery = 75% Analysis Date = 11/22/16 Pct Recovery = 75% Analysis Date = 11/18/16 Pct Recovery = 75% Analysis Date = 11/18/16 Pct Recovery = 75% Analysis Date = 11/13/16 Pct Recovery = 75% Analysis Date = 11/13/16 Pct Recovery = 75% Analysis Date = 11/08/16 Pct Recovery = 76% Analysis Date = 11/08/16 Pct Recovery = 76% Analysis Date = 11/03/16 Pct Recovery = 76% Analysis Date = 11/03/16 Pct Recovery = 76% Analysis Date = 10/29/16 Pct Recovery = 77% Analysis Date = 10/29/16 Pct Recovery = 77% Analysis Date = 10/25/16 Pct Recovery = 77% Analysis Date = 10/25/16 Pct Recovery = 77% Analysis Date = 10/20/16 Pct Recovery = 78% Analysis Date = 10/20/16 Pct Recovery = 78% Analysis Date = 10/15/16 Pct Recovery = 78% Analysis Date = 10/15/16 Pct Recovery = 78% Analysis Date = 10/10/16 Pct Recovery = 78% Analysis Date = 10/10/16 Pct Recovery = 78% Analysis Date = 10/06/16 Pct Recovery = 79% Analysis Date = 10/06/16 Pct Recovery = 79% Analysis Date = 10/01/16 Pct Recovery = 79% Analysis Date = 10/01/16 Pct Recovery = 79% Analysis Date = 09/26/16 Pct Recovery = 80% Analysis Date = 09/26/16 Pct Recovery = 80% Analysis Date = 09/21/16 Pct Recovery = 80% Analysis Date = 09/21/16 Pct Recovery = 80% Analysis Date = 09/16/16 Pct Recovery = 81% Analysis Date = 09/16/16 Pct Recovery = 81% Analysis Date = 09/12/16 Pct Recovery = 81% Analysis Date = 09/12/16 Pct Recovery = 81% Analysis Date = 09/07/16 Pct Recovery = 82% Analysis Date = 09/07/16 Pct Recovery = 82% Analysis Date = 09/02/16 Pct Recovery = 82% Analysis Date = 09/02/16 Pct Recovery = 82% Analysis Date = 08/28/16 Pct Recovery = 82% Analysis Date = 08/28/16 Pct Recovery = 82% Analysis Date = 08/24/16 Pct Recovery = 83% Analysis Date = 08/24/16 Pct Recovery = 83% Analysis Date = 08/19/16 Pct Recovery = 83% Analysis Date = 08/19/16 Pct Recovery = 83% Analysis Date = 08/14/16 Pct Recovery = 84% Analysis Date = 08/14/16 Pct Recovery = 84% Analysis Date = 08/09/16 Pct Recovery = 84% Analysis Date = 08/09/16 Pct Recovery = 84% Analysis Date = 08/04/16 Pct Recovery = 85% Analysis Date = 08/04/16 Pct Recovery = 85% Analysis Date = 07/31/16 Pct Recovery = 85% Analysis Date = 07/31/16 Pct Recovery = 85% Analysis Date = 07/26/16 Pct Recovery = 85% Analysis Date = 07/26/16 Pct Recovery = 85% Analysis Date = 07/21/16 Pct Recovery = 86% Analysis Date = 07/21/16 Pct Recovery = 86% Analysis Date = 07/16/16 Pct Recovery = 86% Analysis Date = 07/16/16 Pct Recovery = 86% Analysis Date = 07/12/16 Pct Recovery = 87% Analysis Date = 07/12/16 Pct Recovery = 87% Analysis Date = 07/07/16 Pct Recovery = 87% Analysis Date = 07/07/16 Pct Recovery = 87% Analysis Date = 07/02/16 Pct Recovery = 87% Analysis Date = 07/02/16 Pct Recovery = 87% Analysis Date = 06/27/16 Pct Recovery = 88% Analysis Date = 06/27/16 Pct Recovery = 88% Analysis Date = 06/22/16 Pct Recovery = 88% Analysis Date = 06/22/16 Pct Recovery = 88% Analysis Date = 06/18/16 Pct Recovery = 89% Analysis Date = 06/18/16 Pct Recovery = 89% Analysis Date = 06/13/16 Pct Recovery = 89% Analysis Date = 06/13/16 Pct Recovery = 89% Analysis Date = 06/08/16 Pct Recovery = 89% Analysis Date = 06/08/16 Pct Recovery = 89% Analysis Date = 06/03/16 Pct Recovery = 90% Analysis Date = 06/03/16 Pct Recovery = 90% Analysis Date = 05/30/16 Pct Recovery = 90% Analysis Date = 05/30/16 Pct Recovery = 90% Analysis Date = 05/25/16 Pct Recovery = 91% Analysis Date = 05/25/16 Pct Recovery = 91% Analysis Date = 05/20/16 Pct Recovery = 91% Analysis Date = 05/20/16 Pct Recovery = 91% Analysis Date = 05/15/16 Pct Recovery = 91% Analysis Date = 05/15/16 Pct Recovery = 91% Analysis Date = 05/10/16 Pct Recovery = 92% Analysis Date = 05/10/16 Pct Recovery = 92% Analysis Date = 05/06/16 Pct Recovery = 92% Analysis Date = 05/06/16 Pct Recovery = 92% Analysis Date = 05/01/16 Pct Recovery = 93% Analysis Date = 05/01/16 Pct Recovery = 93% Analysis Date = 04/26/16 Pct Recovery = 93% Analysis Date = 04/26/16 Pct Recovery = 93% Analysis Date = 04/21/16 Pct Recovery = 93% Analysis Date = 04/21/16 Pct Recovery = 93% Analysis Date = 04/16/16 Pct Recovery = 94% Analysis Date = 04/16/16 Pct Recovery = 94% Analysis Date = 04/12/16 Pct Recovery = 94% Analysis Date = 04/12/16 Pct Recovery = 94% Analysis Date = 04/07/16 Pct Recovery = 95% Analysis Date = 04/07/16 Pct Recovery = 95% Analysis Date = 04/02/16 Pct Recovery = 95% Analysis Date = 04/02/16 Pct Recovery = 95% Analysis Date = 03/28/16 Pct Recovery = 95% Analysis Date = 03/28/16 Pct Recovery = 95% Analysis Date = 03/24/16 Pct Recovery = 96% Analysis Date = 03/24/16 Pct Recovery = 96% Analysis Date = 03/19/16 Pct Recovery = 96% Analysis Date = 03/19/16 Pct Recovery = 96% Analysis Date = 03/14/16 Pct Recovery = 96% Analysis Date = 03/14/16 Pct Recovery = 96% Analysis Date = 03/09/16 Pct Recovery = 97% Analysis Date = 03/09/16 Pct Recovery = 97% Analysis Date = 03/04/16 Pct Recovery = 97% Analysis Date = 03/04/16 Pct Recovery = 97% Analysis Date = 02/29/16 Pct Recovery = 97% Analysis Date = 02/29/16 Pct Recovery = 97% Analysis Date = 02/24/16 Pct Recovery = 98% Analysis Date = 02/24/16 Pct Recovery = 98% Analysis Date = 02/19/16 Pct Recovery = 98% Analysis Date = 02/19/16 Pct Recovery = 98% Analysis Date = 02/14/16 Pct Recovery = 98% Analysis Date = 02/14/16 Pct Recovery = 98% Analysis Date = 02/10/16 Pct Recovery = 99% Analysis Date = 02/10/16 Pct Recovery = 99% Analysis Date = 02/05/16 Pct Recovery = 99% Analysis Date = 02/05/16 Pct Recovery = 99% Analysis Date = 01/31/16 Pct Recovery = 99% Analysis Date = 01/31/16 Pct Recovery = 99% Analysis Date = 01/26/16 Pct Recovery = 100% Analysis Date = 01/26/16 Pct Recovery = 100% Analysis Date = 01/21/16 Pct Recovery = 100% Analysis Date = 01/21/16 Pct Recovery = 100% Analysis Date = 01/17/16 Pct Recovery = 100% Analysis Date = 01/17/16 Pct Recovery = 100% Analysis Date = 01/12/16 Pct Recovery = 101% Analysis Date = 01/12/16 Pct Recovery = 101% Analysis Date = 01/07/16 Pct Recovery = 101% Analysis Date = 01/07/16 Pct Recovery = 101% Analysis Date = 01/02/16 Pct Recovery = 101% Analysis Date = 01/02/16 Pct Recovery = 101% Analysis Date = 12/29/15 Pct Recovery = 102% Analysis Date = 12/29/15 Pct Recovery = 102% Analysis Date = 12/24/15 Pct Recovery = 102% Analysis Date = 12/24/15 Pct Recovery = 102% Analysis Date = 12/19/15 Pct Recovery = 102% Analysis Date = 12/19/15 Pct Recovery = 102% Analysis Date = 12/14/15 Pct Recovery = 103% Analysis Date = 12/14/15 Pct Recovery = 103% Analysis Date = 12/09/15 Pct Recovery = 103% Analysis Date = 12/09/15 Pct Recovery = 103% Analysis Date = 12/05/15 Pct Recovery = 103% Analysis Date = 12/05/15 Pct Recovery = 103% Analysis Date = 11/30/15 Pct Recovery = 104% Analysis Date = 11/30/15 Pct Recovery = 104% Analysis Date = 11/25/15 Pct Recovery = 104% Analysis Date = 11/25/15 Pct Recovery = 104% Analysis Date = 11/20/15 Pct Recovery = 104% Analysis Date = 11/20/15 Pct Recovery = 104% Analysis Date = 11/16/15 Pct Recovery = 104% Analysis Date = 11/16/15 Pct Recovery = 104% Analysis Date = 11/11/15 Pct Recovery = 105% Analysis Date = 11/11/15 Pct Recovery = 105% Analysis Date = 11/06/15 Pct Recovery = 105% Analysis Date = 11/06/15 Pct Recovery = 105% Analysis Date = 11/01/15 Pct Recovery = 105% Analysis Date = 11/01/15 Pct Recovery = 105% Analysis Date = 10/27/15 Pct Recovery = 105% Analysis Date = 10/27/15 Pct Recovery = 105% Analysis Date = 10/23/15 Pct Recovery = 105% Analysis Date = 10/23/15 Pct Recovery = 105% Analysis Date = 10/18/15 Pct Recovery = 106% Analysis Date = 10/18/15 Pct Recovery = 106% Analysis Date = 10/13/15 Pct Recovery = 106% Analysis Date = 10/13/15 Pct Recovery = 106% Analysis Date = 10/08/15 Pct Recovery = 106% Analysis Date = 10/08/15 Pct Recovery = 106% Analysis Date = 10/04/15 Pct Recovery = 106% Analysis Date = 10/04/15 Pct Recovery = 106% Analysis Date = 09/29/15 Pct Recovery = 106% Analysis Date = 09/29/15 Pct Recovery = 106% Analysis Date = 09/24/15 Pct Recovery = 106% Analysis Date = 09/24/15 Pct Recovery = 106% Analysis Date = 09/19/15 Pct Recovery = 106% Analysis Date = 09/19/15 Pct Recovery = 106% Analysis Date = 09/14/15 Pct Recovery = 106% Analysis Date = 09/14/15 Pct Recovery = 106% Analysis Date = 09/10/15 Pct Recovery = 106% Analysis Date = 09/10/15 Pct Recovery = 106% Analysis Date = 09/05/15 Pct Recovery = 106% Analysis Date = 09/05/15 Pct Recovery = 106% Analysis Date = 08/31/15 Pct Recovery = 106% Analysis Date = 08/31/15 Pct Recovery = 106% Analysis Date = 08/26/15 Pct Recovery = 106% Analysis Date = 08/26/15 Pct Recovery = 106% Analysis Date = 08/21/15 Pct Recovery = 106% Analysis Date = 08/21/15 Pct Recovery = 106% Analysis Date = 08/17/15 Pct Recovery = 106% Analysis Date = 08/17/15 Pct Recovery = 106% Analysis Date = 08/12/15 Pct Recovery = 106% Analysis Date = 08/12/15 Pct Recovery = 106% Analysis Date = 08/07/15 Pct Recovery = 106% Analysis Date = 08/07/15 Pct Recovery = 106% Analysis Date = 08/02/15 Pct Recovery = 106% Analysis Date = 08/02/15 Pct Recovery = 106% Analysis Date = 07/29/15 Pct Recovery = 106% Analysis Date = 07/29/15 Pct Recovery = 106% Analysis Date = 07/24/15 Pct Recovery = 106% Analysis Date = 07/24/15 Pct Recovery = 106% Analysis Date = 07/19/15 Pct Recovery = 106% Analysis Date = 07/19/15 Pct Recovery = 106% Analysis Date = 07/14/15 Pct Recovery = 106% Analysis Date = 07/14/15 Pct Recovery = 106% Analysis Date = 07/09/15 Pct Recovery = 106% Analysis Date = 07/09/15 Pct Recovery = 106% Analysis Date = 07/05/15 Pct Recovery = 106% Analysis Date = 07/05/15 Pct Recovery = 106% Analysis Date = 06/30/15 Pct Recovery = 106% Analysis Date = 06/30/15 Pct Recovery = 106% Analysis Date = 06/25/15 Pct Recovery = 106% Analysis Date = 06/25/15 Pct Recovery = 106% Analysis Date = 06/20/15 Pct Recovery = 106% Analysis Date = 06/20/15 Pct Recovery = 106% Analysis Date = 06/16/15 Pct Recovery = 106% Analysis Date = 06/16/15 Pct Recovery = 106% Analysis Date = 06/11/15 Pct Recovery = 106% Analysis Date = 06/11/15 Pct Recovery = 106% Analysis Date = 06/06/15 Pct Recovery = 106% Analysis Date = 06/06/15 Pct Recovery = 106% Analysis Date = 06/01/15 Pct Recovery = 105% Analysis Date = 06/01/15 Pct Recovery = 105% Analysis Date = 05/27/15 Pct Recovery = 105% Analysis Date = 05/27/15 Pct Recovery = 105% Analysis Date = 05/23/15 Pct Recovery = 105% Analysis Date = 05/23/15 Pct Recovery = 105% Analysis Date = 05/18/15 Pct Recovery = 105% Analysis Date = 05/18/15 Pct Recovery = 105% Analysis Date = 05/13/15 Pct Recovery = 105% Analysis Date = 05/13/15 Pct Recovery = 105% Analysis Date = 05/08/15 Pct Recovery = 105% Analysis Date = 05/08/15 Pct Recovery = 105% Analysis Date = 05/04/15 Pct Recovery = 105% Analysis Date = 05/04/15 Pct Recovery = 105% Analysis Date = 04/29/15 Pct Recovery = 105% Analysis Date = 04/29/15 Pct Recovery = 105% Analysis Date = 04/24/15 Pct Recovery = 104% Analysis Date = 04/24/15 Pct Recovery = 104% Analysis Date = 04/19/15 Pct Recovery = 104% Analysis Date = 04/19/15 Pct Recovery = 104% Analysis Date = 04/14/15 Pct Recovery = 104% Analysis Date = 04/14/15 Pct Recovery = 104% Analysis Date = 04/10/15 Pct Recovery = 104% Analysis Date = 04/10/15 Pct Recovery = 104% Analysis Date = 04/05/15 Pct Recovery = 104% Analysis Date = 04/05/15 Pct Recovery = 104% Analysis Date = 03/31/15 Pct Recovery = 104% Analysis Date = 03/31/15 Pct Recovery = 104% Analysis Date = 03/26/15 Pct Recovery = 104% Analysis Date = 03/26/15 Pct Recovery = 104% Analysis Date = 03/22/15 Pct Recovery = 104% Analysis Date = 03/22/15 Pct Recovery = 104% Analysis Date = 03/17/15 Pct Recovery = 104% Analysis Date = 03/17/15 Pct Recovery = 104% Analysis Date = 03/12/15 Pct Recovery = 104% Analysis Date = 03/12/15 Pct Recovery = 104% Analysis Date = 03/07/15 Pct Recovery = 105% Analysis Date = 03/07/15 Pct Recovery = 105% Analysis Date = 03/02/15 Pct Recovery = 105% Analysis Date = 03/02/15 Pct Recovery = 105% Analysis Date = 02/26/15 Pct Recovery = 105% Analysis Date = 02/26/15 Pct Recovery = 105% Analysis Date = 02/21/15 Pct Recovery = 105% Analysis Date = 02/21/15 Pct Recovery = 105% Analysis Date = 02/16/15 Pct Recovery = 105% Analysis Date = 02/16/15 Pct Recovery = 105% Analysis Date = 02/11/15 Pct Recovery = 105% Analysis Date = 02/11/15 Pct Recovery = 105% Analysis Date = 02/07/15 Pct Recovery = 105% Analysis Date = 02/07/15 Pct Recovery = 105% Analysis Date = 02/02/15 Pct Recovery = 105% Analysis Date = 02/02/15 Pct Recovery = 105% Analysis Date = 01/28/15 Pct Recovery = 105% Analysis Date = 01/28/15 Pct Recovery = 105% Analysis Date = 01/23/15 Pct Recovery = 105% Analysis Date = 01/23/15 Pct Recovery = 105% Analysis Date = 01/18/15 Pct Recovery = 105% Analysis Date = 01/18/15 Pct Recovery = 105% Analysis Date = 01/14/15 Pct Recovery = 105% Analysis Date = 01/14/15 Pct Recovery = 105% Analysis Date = 01/09/15 Pct Recovery = 106% Analysis Date = 01/09/15 Pct Recovery = 106% Analysis Date = 01/04/15 Pct Recovery = 106% Analysis Date = 01/04/15 Pct Recovery = 106% Analysis Date = 12/30/14 Pct Recovery = 106% Analysis Date = 12/30/14 Pct Recovery = 106% Analysis Date = 12/25/14 Pct Recovery = 106% Analysis Date = 12/25/14 Pct Recovery = 106% Analysis Date = 12/21/14 Pct Recovery = 106% Analysis Date = 12/21/14 Pct Recovery = 106% Analysis Date = 12/16/14 Pct Recovery = 106% Analysis Date = 12/16/14 Pct Recovery = 106% Analysis Date = 12/11/14 Pct Recovery = 106% Analysis Date = 12/11/14 Pct Recovery = 106% Analysis Date = 12/06/14 Pct Recovery = 106% Analysis Date = 12/06/14 Pct Recovery = 106% Analysis Date = 12/02/14 Pct Recovery = 106% Analysis Date = 12/02/14 Pct Recovery = 106% Analysis Date = 11/27/14 Pct Recovery = 106% Analysis Date = 11/27/14 Pct Recovery = 106% Analysis Date = 11/22/14 Pct Recovery = 106% Analysis Date = 11/22/14 Pct Recovery = 106% Analysis Date = 11/17/14 Pct Recovery = 106% Analysis Date = 11/17/14 Pct Recovery = 106% Analysis Date = 11/12/14 Pct Recovery = 107% Analysis Date = 11/12/14 Pct Recovery = 107% Analysis Date = 11/08/14 Pct Recovery = 107% Analysis Date = 11/08/14 Pct Recovery = 107% Analysis Date = 11/03/14 Pct Recovery = 107% Analysis Date = 11/03/14 Pct Recovery = 107% Analysis Date = 10/29/14 Pct Recovery = 107% Analysis Date = 10/29/14 Pct Recovery = 107% Analysis Date = 10/24/14 Pct Recovery = 107% Analysis Date = 10/24/14 Pct Recovery = 107% Analysis Date = 10/20/14 Pct Recovery = 107% Analysis Date = 10/20/14 Pct Recovery = 107% Analysis Date = 10/15/14 Pct Recovery = 107% Analysis Date = 10/15/14 Pct Recovery = 107% Analysis Date = 10/10/14 Pct Recovery = 107% Analysis Date = 10/10/14 Pct Recovery = 107% Analysis Date = 10/05/14 Pct Recovery = 108% Analysis Date = 10/05/14 Pct Recovery = 108% Analysis Date = 09/30/14 Pct Recovery = 108% Analysis Date = 09/30/14 Pct Recovery = 108% Analysis Date = 09/26/14 Pct Recovery = 108% Analysis Date = 09/26/14 Pct Recovery = 108% Analysis Date = 09/21/14 Pct Recovery = 108% Analysis Date = 09/21/14 Pct Recovery = 108% Analysis Date = 09/16/14 Pct Recovery = 108% Analysis Date = 09/16/14 Pct Recovery = 108% Analysis Date = 09/11/14 Pct Recovery = 108% Analysis Date = 09/11/14 Pct Recovery = 108% Analysis Date = 09/07/14 Pct Recovery = 108% Analysis Date = 09/07/14 Pct Recovery = 108% Analysis Date = 09/02/14 Pct Recovery = 109% Analysis Date = 09/02/14 Pct Recovery = 109% Analysis Date = 08/28/14 Pct Recovery = 109% Analysis Date = 08/28/14 Pct Recovery = 109% Analysis Date = 08/23/14 Pct Recovery = 109% Analysis Date = 08/23/14 Pct Recovery = 109% Analysis Date = 08/18/14 Pct Recovery = 109% Analysis Date = 08/18/14 Pct Recovery = 109% Analysis Date = 08/14/14 Pct Recovery = 109% Analysis Date = 08/14/14 Pct Recovery = 109% Analysis Date = 08/09/14 Pct Recovery = 109% Analysis Date = 08/09/14 Pct Recovery = 109% Analysis Date = 08/04/14 Pct Recovery = 109% Analysis Date = 08/04/14 Pct Recovery = 109% Analysis Date = 07/30/14 Pct Recovery = 110% Analysis Date = 07/30/14 Pct Recovery = 110% Analysis Date = 07/26/14 Pct Recovery = 110% Analysis Date = 07/26/14 Pct Recovery = 110% Analysis Date = 07/21/14 Pct Recovery = 110% Analysis Date = 07/21/14 Pct Recovery = 110% Analysis Date = 07/16/14 Pct Recovery = 110% Analysis Date = 07/16/14 Pct Recovery = 110% Analysis Date = 07/11/14 Pct Recovery = 110% Analysis Date = 07/11/14 Pct Recovery = 110% Analysis Date = 07/06/14 Pct Recovery = 110% Analysis Date = 07/06/14 Pct Recovery = 110% Analysis Date = 07/02/14 Pct Recovery = 111% Analysis Date = 07/02/14 Pct Recovery = 111% Analysis Date = 06/27/14 Pct Recovery = 111% Analysis Date = 06/27/14 Pct Recovery = 111% Analysis Date = 06/22/14 Pct Recovery = 111% Analysis Date = 06/22/14 Pct Recovery = 111% Analysis Date = 06/17/14 Pct Recovery = 111% Analysis Date = 06/17/14 Pct Recovery = 111% Analysis Date = 06/13/14 Pct Recovery = 111% Analysis Date = 06/13/14 Pct Recovery = 111% Analysis Date = 06/08/14 Pct Recovery = 112% Analysis Date = 06/08/14 Pct Recovery = 112% Analysis Date = 06/03/14 Pct Recovery = 112% Analysis Date = 06/03/14 Pct Recovery = 112% Analysis Date = 05/29/14 Pct Recovery = 112% Analysis Date = 05/29/14 Pct Recovery = 112% Analysis Date = 05/24/14 Pct Recovery = 112% Analysis Date = 05/24/14 Pct Recovery = 112% Analysis Date = 05/20/14 Pct Recovery = 113% Analysis Date = 05/20/14 Pct Recovery = 113% Analysis Date = 05/15/14 Pct Recovery = 113% Analysis Date = 05/15/14 Pct Recovery = 113% Analysis Date = 05/10/14 Pct Recovery = 113% Analysis Date = 05/10/14 Pct Recovery = 113% Analysis Date = 05/05/14 Pct Recovery = 113% Analysis Date = 05/05/14 Pct Recovery = 113% Analysis Date = 05/01/14 Pct Recovery = 113% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
CHLORODIFLUOROMETHANE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 7 92% 13% 92% 13%
>= Reporting Level 35 103% 19% 105% 19%
Total 42 101% 18% 103% 16%

Sample Statistics
CHLORODIFLUOROMETHANE

Characteristic N % % Basis
Plotted 42 100% Spiked
Estimated Values 1 2% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 42 .  
False Negatives 0 0% 0 out of 42
Not Spiked 31 .  
False Positives 0 0% 0 out of 31

BQS OBSP Determination:
CHLOROETHANE
METHOD: 4440 , TESTIDCODE: 34311GCM66
Open Data Set

Analysis Date = 12/12/16 SpikeMix = Accu 216041125: 40 µl & Crescent 03FF058: 40 µl Pct Recovery = 87% Analysis Date = 07/20/16 SpikeMix = Supelco LC20141V: 40 µl & Accu 216041125: 40 µl Pct Recovery = 99% Analysis Date = 07/14/16 SpikeMix = Accu 216041125: 40 µl & NSI 041816AVOC: 40 µl Pct Recovery = 82% Analysis Date = 09/08/16 SpikeMix = Supelco LC20141V: 25 µl & Accu 216041125: 25 µl Pct Recovery = 86% Analysis Date = 05/24/16 SpikeMix = Accu 216041125: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 88% Analysis Date = 08/12/16 SpikeMix = ChemService 5082900: 25 µl & Phenova B20160319: 25 µl Pct Recovery = 95% Analysis Date = 06/21/16 SpikeMix = Phenova B20160319: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 98% Analysis Date = 04/09/15 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 108% Analysis Date = 02/28/15 SpikeMix = ERA 0227-14-06.1A: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 120% Analysis Date = 11/22/14 SpikeMix = NSI 032614: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 112% Analysis Date = 11/14/14 SpikeMix = Crescent 03DD004: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 96% Analysis Date = 08/16/14 SpikeMix = ERA 0227-14-06.1A: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 125% Analysis Date = 07/01/14 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 114% Analysis Date = 06/10/14 SpikeMix = Crescent 03DD004: 20 µl & NSI 032614: 20 µl Pct Recovery = 96% Analysis Date = 06/10/14 SpikeMix = NSI 032614: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 103% Analysis Date = 05/01/14 SpikeMix = Accu 214031115: 20 µl & NSI 032614: 20 µl Pct Recovery = 105% Analysis Date = 09/29/15 SpikeMix = Accu 215041380: 25 µl & ERA 0406-15-03: 25 µl Pct Recovery = 65% Analysis Date = 08/15/15 SpikeMix = Supelco LC13545: 25 µl & Crescent 04EE008: 25 µl Pct Recovery = 106% Analysis Date = 07/13/15 SpikeMix = Crescent 04EE008: 25 µl & NSI 050515AVOC: 25 µl Pct Recovery = 92% Analysis Date = 10/13/16 SpikeMix = Accu 216041125: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 101% Analysis Date = 08/20/16 SpikeMix = Accu 216041125: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 99% Analysis Date = 06/30/16 SpikeMix = ChemService 5082900: 15 µl & Accu 216041125: 15 µl Pct Recovery = 75% Analysis Date = 11/29/16 SpikeMix = ChemService 5082900: 15 µl & Phenova B20160319: 15 µl Pct Recovery = 113% Analysis Date = 09/08/16 SpikeMix = Phenova B20160319: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 105% Analysis Date = 07/29/16 SpikeMix = Phenova B20160319: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 111% Analysis Date = 05/27/16 SpikeMix = Phenova B20160319: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 94% Analysis Date = 04/02/16 SpikeMix = Supelco LC13545: 15 µl & Accu 215041380: 15 µl Pct Recovery = 85% Analysis Date = 03/04/16 SpikeMix = Accu 215041380: 15 µl & ERA 0406-15-03: 15 µl Pct Recovery = 71% Analysis Date = 06/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Accu 215041380: 15 µl Pct Recovery = 79% Analysis Date = 12/18/15 SpikeMix = Supelco LC13545: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 99% Analysis Date = 10/17/15 SpikeMix = Crescent 04EE008: 15 µl & NSI 050515AVOC: 15 µl Pct Recovery = 91% Analysis Date = 05/09/15 SpikeMix = Spex Organics EN150428007: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 87% Analysis Date = 01/13/15 SpikeMix = Accu 214031115: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 125% Analysis Date = 10/21/14 SpikeMix = ERA 0227-14-06.1A: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 117% Analysis Date = 10/04/14 SpikeMix = Crescent 03DD004: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 121% Analysis Date = 09/09/14 SpikeMix = Accu 214031115: 10 µl & NSI 032614: 10 µl Pct Recovery = 122% Analysis Date = 09/09/14 SpikeMix = NSI 032614: 10 µl & Spex Organics C1140417015: 10 µl Pct Recovery = 118% Analysis Date = 07/29/14 SpikeMix = Crescent 03DD004: 10 µl & NSI 032614: 10 µl Pct Recovery = 115% Analysis Date = 07/11/14 SpikeMix = Spex Organics C1140417015: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 101% Analysis Date = 02/18/16 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 66% Analysis Date = 11/20/15 SpikeMix = Accu 215041380: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 84% Analysis Date = 11/12/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 81% Analysis Date = 05/21/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 62% Analysis Date = 05/13/16 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 93% Analysis Date = 01/27/16 SpikeMix = Crescent 04EE008: 10 µl & NSI 050515AVOC: 10 µl Pct Recovery = 116% Analysis Date = 07/31/15 SpikeMix = Crescent 04EE008: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 83% Analysis Date = 05/09/15 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 93% Analysis Date = 12/11/16 Pct Recovery = 100% Analysis Date = 12/07/16 Pct Recovery = 100% Analysis Date = 12/07/16 Pct Recovery = 100% Analysis Date = 12/02/16 Pct Recovery = 100% Analysis Date = 12/02/16 Pct Recovery = 100% Analysis Date = 11/27/16 Pct Recovery = 100% Analysis Date = 11/27/16 Pct Recovery = 100% Analysis Date = 11/22/16 Pct Recovery = 99% Analysis Date = 11/22/16 Pct Recovery = 99% Analysis Date = 11/18/16 Pct Recovery = 99% Analysis Date = 11/18/16 Pct Recovery = 99% Analysis Date = 11/13/16 Pct Recovery = 99% Analysis Date = 11/13/16 Pct Recovery = 99% Analysis Date = 11/08/16 Pct Recovery = 99% Analysis Date = 11/08/16 Pct Recovery = 99% Analysis Date = 11/03/16 Pct Recovery = 99% Analysis Date = 11/03/16 Pct Recovery = 99% Analysis Date = 10/29/16 Pct Recovery = 98% Analysis Date = 10/29/16 Pct Recovery = 98% Analysis Date = 10/25/16 Pct Recovery = 98% Analysis Date = 10/25/16 Pct Recovery = 98% Analysis Date = 10/20/16 Pct Recovery = 98% Analysis Date = 10/20/16 Pct Recovery = 98% Analysis Date = 10/15/16 Pct Recovery = 98% Analysis Date = 10/15/16 Pct Recovery = 98% Analysis Date = 10/10/16 Pct Recovery = 98% Analysis Date = 10/10/16 Pct Recovery = 98% Analysis Date = 10/06/16 Pct Recovery = 97% Analysis Date = 10/06/16 Pct Recovery = 97% Analysis Date = 10/01/16 Pct Recovery = 97% Analysis Date = 10/01/16 Pct Recovery = 97% Analysis Date = 09/26/16 Pct Recovery = 97% Analysis Date = 09/26/16 Pct Recovery = 97% Analysis Date = 09/21/16 Pct Recovery = 97% Analysis Date = 09/21/16 Pct Recovery = 97% Analysis Date = 09/16/16 Pct Recovery = 96% Analysis Date = 09/16/16 Pct Recovery = 96% Analysis Date = 09/12/16 Pct Recovery = 96% Analysis Date = 09/12/16 Pct Recovery = 96% Analysis Date = 09/07/16 Pct Recovery = 96% Analysis Date = 09/07/16 Pct Recovery = 96% Analysis Date = 09/02/16 Pct Recovery = 96% Analysis Date = 09/02/16 Pct Recovery = 96% Analysis Date = 08/28/16 Pct Recovery = 96% Analysis Date = 08/28/16 Pct Recovery = 96% Analysis Date = 08/24/16 Pct Recovery = 95% Analysis Date = 08/24/16 Pct Recovery = 95% Analysis Date = 08/19/16 Pct Recovery = 95% Analysis Date = 08/19/16 Pct Recovery = 95% Analysis Date = 08/14/16 Pct Recovery = 95% Analysis Date = 08/14/16 Pct Recovery = 95% Analysis Date = 08/09/16 Pct Recovery = 95% Analysis Date = 08/09/16 Pct Recovery = 95% Analysis Date = 08/04/16 Pct Recovery = 95% Analysis Date = 08/04/16 Pct Recovery = 95% Analysis Date = 07/31/16 Pct Recovery = 94% Analysis Date = 07/31/16 Pct Recovery = 94% Analysis Date = 07/26/16 Pct Recovery = 94% Analysis Date = 07/26/16 Pct Recovery = 94% Analysis Date = 07/21/16 Pct Recovery = 94% Analysis Date = 07/21/16 Pct Recovery = 94% Analysis Date = 07/16/16 Pct Recovery = 94% Analysis Date = 07/16/16 Pct Recovery = 94% Analysis Date = 07/12/16 Pct Recovery = 94% Analysis Date = 07/12/16 Pct Recovery = 94% Analysis Date = 07/07/16 Pct Recovery = 93% Analysis Date = 07/07/16 Pct Recovery = 93% Analysis Date = 07/02/16 Pct Recovery = 93% Analysis Date = 07/02/16 Pct Recovery = 93% Analysis Date = 06/27/16 Pct Recovery = 93% Analysis Date = 06/27/16 Pct Recovery = 93% Analysis Date = 06/22/16 Pct Recovery = 93% Analysis Date = 06/22/16 Pct Recovery = 93% Analysis Date = 06/18/16 Pct Recovery = 93% Analysis Date = 06/18/16 Pct Recovery = 93% Analysis Date = 06/13/16 Pct Recovery = 92% Analysis Date = 06/13/16 Pct Recovery = 92% Analysis Date = 06/08/16 Pct Recovery = 92% Analysis Date = 06/08/16 Pct Recovery = 92% Analysis Date = 06/03/16 Pct Recovery = 92% Analysis Date = 06/03/16 Pct Recovery = 92% Analysis Date = 05/30/16 Pct Recovery = 92% Analysis Date = 05/30/16 Pct Recovery = 92% Analysis Date = 05/25/16 Pct Recovery = 92% Analysis Date = 05/25/16 Pct Recovery = 92% Analysis Date = 05/20/16 Pct Recovery = 91% Analysis Date = 05/20/16 Pct Recovery = 91% Analysis Date = 05/15/16 Pct Recovery = 91% Analysis Date = 05/15/16 Pct Recovery = 91% Analysis Date = 05/10/16 Pct Recovery = 91% Analysis Date = 05/10/16 Pct Recovery = 91% Analysis Date = 05/06/16 Pct Recovery = 91% Analysis Date = 05/06/16 Pct Recovery = 91% Analysis Date = 05/01/16 Pct Recovery = 91% Analysis Date = 05/01/16 Pct Recovery = 91% Analysis Date = 04/26/16 Pct Recovery = 91% Analysis Date = 04/26/16 Pct Recovery = 91% Analysis Date = 04/21/16 Pct Recovery = 90% Analysis Date = 04/21/16 Pct Recovery = 90% Analysis Date = 04/16/16 Pct Recovery = 90% Analysis Date = 04/16/16 Pct Recovery = 90% Analysis Date = 04/12/16 Pct Recovery = 90% Analysis Date = 04/12/16 Pct Recovery = 90% Analysis Date = 04/07/16 Pct Recovery = 90% Analysis Date = 04/07/16 Pct Recovery = 90% Analysis Date = 04/02/16 Pct Recovery = 90% Analysis Date = 04/02/16 Pct Recovery = 90% Analysis Date = 03/28/16 Pct Recovery = 90% Analysis Date = 03/28/16 Pct Recovery = 90% Analysis Date = 03/24/16 Pct Recovery = 89% Analysis Date = 03/24/16 Pct Recovery = 89% Analysis Date = 03/19/16 Pct Recovery = 89% Analysis Date = 03/19/16 Pct Recovery = 89% Analysis Date = 03/14/16 Pct Recovery = 89% Analysis Date = 03/14/16 Pct Recovery = 89% Analysis Date = 03/09/16 Pct Recovery = 89% Analysis Date = 03/09/16 Pct Recovery = 89% Analysis Date = 03/04/16 Pct Recovery = 89% Analysis Date = 03/04/16 Pct Recovery = 89% Analysis Date = 02/29/16 Pct Recovery = 89% Analysis Date = 02/29/16 Pct Recovery = 89% Analysis Date = 02/24/16 Pct Recovery = 88% Analysis Date = 02/24/16 Pct Recovery = 88% Analysis Date = 02/19/16 Pct Recovery = 88% Analysis Date = 02/19/16 Pct Recovery = 88% Analysis Date = 02/14/16 Pct Recovery = 88% Analysis Date = 02/14/16 Pct Recovery = 88% Analysis Date = 02/10/16 Pct Recovery = 88% Analysis Date = 02/10/16 Pct Recovery = 88% Analysis Date = 02/05/16 Pct Recovery = 88% Analysis Date = 02/05/16 Pct Recovery = 88% Analysis Date = 01/31/16 Pct Recovery = 88% Analysis Date = 01/31/16 Pct Recovery = 88% Analysis Date = 01/26/16 Pct Recovery = 88% Analysis Date = 01/26/16 Pct Recovery = 88% Analysis Date = 01/21/16 Pct Recovery = 88% Analysis Date = 01/21/16 Pct Recovery = 88% Analysis Date = 01/17/16 Pct Recovery = 88% Analysis Date = 01/17/16 Pct Recovery = 88% Analysis Date = 01/12/16 Pct Recovery = 87% Analysis Date = 01/12/16 Pct Recovery = 87% Analysis Date = 01/07/16 Pct Recovery = 87% Analysis Date = 01/07/16 Pct Recovery = 87% Analysis Date = 01/02/16 Pct Recovery = 87% Analysis Date = 01/02/16 Pct Recovery = 87% Analysis Date = 12/29/15 Pct Recovery = 87% Analysis Date = 12/29/15 Pct Recovery = 87% Analysis Date = 12/24/15 Pct Recovery = 87% Analysis Date = 12/24/15 Pct Recovery = 87% Analysis Date = 12/19/15 Pct Recovery = 87% Analysis Date = 12/19/15 Pct Recovery = 87% Analysis Date = 12/14/15 Pct Recovery = 87% Analysis Date = 12/14/15 Pct Recovery = 87% Analysis Date = 12/09/15 Pct Recovery = 87% Analysis Date = 12/09/15 Pct Recovery = 87% Analysis Date = 12/05/15 Pct Recovery = 87% Analysis Date = 12/05/15 Pct Recovery = 87% Analysis Date = 11/30/15 Pct Recovery = 87% Analysis Date = 11/30/15 Pct Recovery = 87% Analysis Date = 11/25/15 Pct Recovery = 87% Analysis Date = 11/25/15 Pct Recovery = 87% Analysis Date = 11/20/15 Pct Recovery = 86% Analysis Date = 11/20/15 Pct Recovery = 86% Analysis Date = 11/16/15 Pct Recovery = 86% Analysis Date = 11/16/15 Pct Recovery = 86% Analysis Date = 11/11/15 Pct Recovery = 87% Analysis Date = 11/11/15 Pct Recovery = 87% Analysis Date = 11/06/15 Pct Recovery = 87% Analysis Date = 11/06/15 Pct Recovery = 87% Analysis Date = 11/01/15 Pct Recovery = 87% Analysis Date = 11/01/15 Pct Recovery = 87% Analysis Date = 10/27/15 Pct Recovery = 87% Analysis Date = 10/27/15 Pct Recovery = 87% Analysis Date = 10/23/15 Pct Recovery = 87% Analysis Date = 10/23/15 Pct Recovery = 87% Analysis Date = 10/18/15 Pct Recovery = 87% Analysis Date = 10/18/15 Pct Recovery = 87% Analysis Date = 10/13/15 Pct Recovery = 87% Analysis Date = 10/13/15 Pct Recovery = 87% Analysis Date = 10/08/15 Pct Recovery = 87% Analysis Date = 10/08/15 Pct Recovery = 87% Analysis Date = 10/04/15 Pct Recovery = 87% Analysis Date = 10/04/15 Pct Recovery = 87% Analysis Date = 09/29/15 Pct Recovery = 87% Analysis Date = 09/29/15 Pct Recovery = 87% Analysis Date = 09/24/15 Pct Recovery = 88% Analysis Date = 09/24/15 Pct Recovery = 88% Analysis Date = 09/19/15 Pct Recovery = 88% Analysis Date = 09/19/15 Pct Recovery = 88% Analysis Date = 09/14/15 Pct Recovery = 88% Analysis Date = 09/14/15 Pct Recovery = 88% Analysis Date = 09/10/15 Pct Recovery = 88% Analysis Date = 09/10/15 Pct Recovery = 88% Analysis Date = 09/05/15 Pct Recovery = 89% Analysis Date = 09/05/15 Pct Recovery = 89% Analysis Date = 08/31/15 Pct Recovery = 89% Analysis Date = 08/31/15 Pct Recovery = 89% Analysis Date = 08/26/15 Pct Recovery = 89% Analysis Date = 08/26/15 Pct Recovery = 89% Analysis Date = 08/21/15 Pct Recovery = 89% Analysis Date = 08/21/15 Pct Recovery = 89% Analysis Date = 08/17/15 Pct Recovery = 89% Analysis Date = 08/17/15 Pct Recovery = 89% Analysis Date = 08/12/15 Pct Recovery = 90% Analysis Date = 08/12/15 Pct Recovery = 90% Analysis Date = 08/07/15 Pct Recovery = 90% Analysis Date = 08/07/15 Pct Recovery = 90% Analysis Date = 08/02/15 Pct Recovery = 90% Analysis Date = 08/02/15 Pct Recovery = 90% Analysis Date = 07/29/15 Pct Recovery = 90% Analysis Date = 07/29/15 Pct Recovery = 90% Analysis Date = 07/24/15 Pct Recovery = 91% Analysis Date = 07/24/15 Pct Recovery = 91% Analysis Date = 07/19/15 Pct Recovery = 91% Analysis Date = 07/19/15 Pct Recovery = 91% Analysis Date = 07/14/15 Pct Recovery = 91% Analysis Date = 07/14/15 Pct Recovery = 91% Analysis Date = 07/09/15 Pct Recovery = 91% Analysis Date = 07/09/15 Pct Recovery = 91% Analysis Date = 07/05/15 Pct Recovery = 92% Analysis Date = 07/05/15 Pct Recovery = 92% Analysis Date = 06/30/15 Pct Recovery = 92% Analysis Date = 06/30/15 Pct Recovery = 92% Analysis Date = 06/25/15 Pct Recovery = 92% Analysis Date = 06/25/15 Pct Recovery = 92% Analysis Date = 06/20/15 Pct Recovery = 93% Analysis Date = 06/20/15 Pct Recovery = 93% Analysis Date = 06/16/15 Pct Recovery = 93% Analysis Date = 06/16/15 Pct Recovery = 93% Analysis Date = 06/11/15 Pct Recovery = 93% Analysis Date = 06/11/15 Pct Recovery = 93% Analysis Date = 06/06/15 Pct Recovery = 94% Analysis Date = 06/06/15 Pct Recovery = 94% Analysis Date = 06/01/15 Pct Recovery = 94% Analysis Date = 06/01/15 Pct Recovery = 94% Analysis Date = 05/27/15 Pct Recovery = 94% Analysis Date = 05/27/15 Pct Recovery = 94% Analysis Date = 05/23/15 Pct Recovery = 95% Analysis Date = 05/23/15 Pct Recovery = 95% Analysis Date = 05/18/15 Pct Recovery = 95% Analysis Date = 05/18/15 Pct Recovery = 95% Analysis Date = 05/13/15 Pct Recovery = 95% Analysis Date = 05/13/15 Pct Recovery = 95% Analysis Date = 05/08/15 Pct Recovery = 96% Analysis Date = 05/08/15 Pct Recovery = 96% Analysis Date = 05/04/15 Pct Recovery = 96% Analysis Date = 05/04/15 Pct Recovery = 96% Analysis Date = 04/29/15 Pct Recovery = 96% Analysis Date = 04/29/15 Pct Recovery = 96% Analysis Date = 04/24/15 Pct Recovery = 97% Analysis Date = 04/24/15 Pct Recovery = 97% Analysis Date = 04/19/15 Pct Recovery = 97% Analysis Date = 04/19/15 Pct Recovery = 97% Analysis Date = 04/14/15 Pct Recovery = 98% Analysis Date = 04/14/15 Pct Recovery = 98% Analysis Date = 04/10/15 Pct Recovery = 98% Analysis Date = 04/10/15 Pct Recovery = 98% Analysis Date = 04/05/15 Pct Recovery = 98% Analysis Date = 04/05/15 Pct Recovery = 98% Analysis Date = 03/31/15 Pct Recovery = 99% Analysis Date = 03/31/15 Pct Recovery = 99% Analysis Date = 03/26/15 Pct Recovery = 99% Analysis Date = 03/26/15 Pct Recovery = 99% Analysis Date = 03/22/15 Pct Recovery = 99% Analysis Date = 03/22/15 Pct Recovery = 99% Analysis Date = 03/17/15 Pct Recovery = 100% Analysis Date = 03/17/15 Pct Recovery = 100% Analysis Date = 03/12/15 Pct Recovery = 100% Analysis Date = 03/12/15 Pct Recovery = 100% Analysis Date = 03/07/15 Pct Recovery = 101% Analysis Date = 03/07/15 Pct Recovery = 101% Analysis Date = 03/02/15 Pct Recovery = 101% Analysis Date = 03/02/15 Pct Recovery = 101% Analysis Date = 02/26/15 Pct Recovery = 101% Analysis Date = 02/26/15 Pct Recovery = 101% Analysis Date = 02/21/15 Pct Recovery = 101% Analysis Date = 02/21/15 Pct Recovery = 101% Analysis Date = 02/16/15 Pct Recovery = 102% Analysis Date = 02/16/15 Pct Recovery = 102% Analysis Date = 02/11/15 Pct Recovery = 102% Analysis Date = 02/11/15 Pct Recovery = 102% Analysis Date = 02/07/15 Pct Recovery = 102% Analysis Date = 02/07/15 Pct Recovery = 102% Analysis Date = 02/02/15 Pct Recovery = 103% Analysis Date = 02/02/15 Pct Recovery = 103% Analysis Date = 01/28/15 Pct Recovery = 103% Analysis Date = 01/28/15 Pct Recovery = 103% Analysis Date = 01/23/15 Pct Recovery = 103% Analysis Date = 01/23/15 Pct Recovery = 103% Analysis Date = 01/18/15 Pct Recovery = 103% Analysis Date = 01/18/15 Pct Recovery = 103% Analysis Date = 01/14/15 Pct Recovery = 104% Analysis Date = 01/14/15 Pct Recovery = 104% Analysis Date = 01/09/15 Pct Recovery = 104% Analysis Date = 01/09/15 Pct Recovery = 104% Analysis Date = 01/04/15 Pct Recovery = 104% Analysis Date = 01/04/15 Pct Recovery = 104% Analysis Date = 12/30/14 Pct Recovery = 104% Analysis Date = 12/30/14 Pct Recovery = 104% Analysis Date = 12/25/14 Pct Recovery = 105% Analysis Date = 12/25/14 Pct Recovery = 105% Analysis Date = 12/21/14 Pct Recovery = 105% Analysis Date = 12/21/14 Pct Recovery = 105% Analysis Date = 12/16/14 Pct Recovery = 105% Analysis Date = 12/16/14 Pct Recovery = 105% Analysis Date = 12/11/14 Pct Recovery = 105% Analysis Date = 12/11/14 Pct Recovery = 105% Analysis Date = 12/06/14 Pct Recovery = 106% Analysis Date = 12/06/14 Pct Recovery = 106% Analysis Date = 12/02/14 Pct Recovery = 106% Analysis Date = 12/02/14 Pct Recovery = 106% Analysis Date = 11/27/14 Pct Recovery = 106% Analysis Date = 11/27/14 Pct Recovery = 106% Analysis Date = 11/22/14 Pct Recovery = 106% Analysis Date = 11/22/14 Pct Recovery = 106% Analysis Date = 11/17/14 Pct Recovery = 107% Analysis Date = 11/17/14 Pct Recovery = 107% Analysis Date = 11/12/14 Pct Recovery = 107% Analysis Date = 11/12/14 Pct Recovery = 107% Analysis Date = 11/08/14 Pct Recovery = 107% Analysis Date = 11/08/14 Pct Recovery = 107% Analysis Date = 11/03/14 Pct Recovery = 107% Analysis Date = 11/03/14 Pct Recovery = 107% Analysis Date = 10/29/14 Pct Recovery = 108% Analysis Date = 10/29/14 Pct Recovery = 108% Analysis Date = 10/24/14 Pct Recovery = 108% Analysis Date = 10/24/14 Pct Recovery = 108% Analysis Date = 10/20/14 Pct Recovery = 108% Analysis Date = 10/20/14 Pct Recovery = 108% Analysis Date = 10/15/14 Pct Recovery = 108% Analysis Date = 10/15/14 Pct Recovery = 108% Analysis Date = 10/10/14 Pct Recovery = 109% Analysis Date = 10/10/14 Pct Recovery = 109% Analysis Date = 10/05/14 Pct Recovery = 109% Analysis Date = 10/05/14 Pct Recovery = 109% Analysis Date = 09/30/14 Pct Recovery = 109% Analysis Date = 09/30/14 Pct Recovery = 109% Analysis Date = 09/26/14 Pct Recovery = 109% Analysis Date = 09/26/14 Pct Recovery = 109% Analysis Date = 09/21/14 Pct Recovery = 109% Analysis Date = 09/21/14 Pct Recovery = 109% Analysis Date = 09/16/14 Pct Recovery = 110% Analysis Date = 09/16/14 Pct Recovery = 110% Analysis Date = 09/11/14 Pct Recovery = 110% Analysis Date = 09/11/14 Pct Recovery = 110% Analysis Date = 09/07/14 Pct Recovery = 110% Analysis Date = 09/07/14 Pct Recovery = 110% Analysis Date = 09/02/14 Pct Recovery = 110% Analysis Date = 09/02/14 Pct Recovery = 110% Analysis Date = 08/28/14 Pct Recovery = 111% Analysis Date = 08/28/14 Pct Recovery = 111% Analysis Date = 08/23/14 Pct Recovery = 111% Analysis Date = 08/23/14 Pct Recovery = 111% Analysis Date = 08/18/14 Pct Recovery = 111% Analysis Date = 08/18/14 Pct Recovery = 111% Analysis Date = 08/14/14 Pct Recovery = 111% Analysis Date = 08/14/14 Pct Recovery = 111% Analysis Date = 08/09/14 Pct Recovery = 111% Analysis Date = 08/09/14 Pct Recovery = 111% Analysis Date = 08/04/14 Pct Recovery = 112% Analysis Date = 08/04/14 Pct Recovery = 112% Analysis Date = 07/30/14 Pct Recovery = 112% Analysis Date = 07/30/14 Pct Recovery = 112% Analysis Date = 07/26/14 Pct Recovery = 112% Analysis Date = 07/26/14 Pct Recovery = 112% Analysis Date = 07/21/14 Pct Recovery = 112% Analysis Date = 07/21/14 Pct Recovery = 112% Analysis Date = 07/16/14 Pct Recovery = 112% Analysis Date = 07/16/14 Pct Recovery = 112% Analysis Date = 07/11/14 Pct Recovery = 113% Analysis Date = 07/11/14 Pct Recovery = 113% Analysis Date = 07/06/14 Pct Recovery = 113% Analysis Date = 07/06/14 Pct Recovery = 113% Analysis Date = 07/02/14 Pct Recovery = 113% Analysis Date = 07/02/14 Pct Recovery = 113% Analysis Date = 06/27/14 Pct Recovery = 113% Analysis Date = 06/27/14 Pct Recovery = 113% Analysis Date = 06/22/14 Pct Recovery = 113% Analysis Date = 06/22/14 Pct Recovery = 113% Analysis Date = 06/17/14 Pct Recovery = 113% Analysis Date = 06/17/14 Pct Recovery = 113% Analysis Date = 06/13/14 Pct Recovery = 114% Analysis Date = 06/13/14 Pct Recovery = 114% Analysis Date = 06/08/14 Pct Recovery = 114% Analysis Date = 06/08/14 Pct Recovery = 114% Analysis Date = 06/03/14 Pct Recovery = 114% Analysis Date = 06/03/14 Pct Recovery = 114% Analysis Date = 05/29/14 Pct Recovery = 114% Analysis Date = 05/29/14 Pct Recovery = 114% Analysis Date = 05/24/14 Pct Recovery = 114% Analysis Date = 05/24/14 Pct Recovery = 114% Analysis Date = 05/20/14 Pct Recovery = 114% Analysis Date = 05/20/14 Pct Recovery = 114% Analysis Date = 05/15/14 Pct Recovery = 115% Analysis Date = 05/15/14 Pct Recovery = 115% Analysis Date = 05/10/14 Pct Recovery = 115% Analysis Date = 05/10/14 Pct Recovery = 115% Analysis Date = 05/05/14 Pct Recovery = 115% Analysis Date = 05/05/14 Pct Recovery = 115% Analysis Date = 05/01/14 Pct Recovery = 115% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
CHLOROETHANE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 47 98% 16% 98% 19%
Total 47 98% 16% 98% 19%

Sample Statistics
CHLOROETHANE

Characteristic N % % Basis
Plotted 47 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 47 .  
False Negatives 0 0% 0 out of 47
Not Spiked 25 .  
False Positives 0 0% 0 out of 25

BQS OBSP Determination:
CHLOROFORM
METHOD: 4440 , TESTIDCODE: 32106GCM66
Open Data Set

Analysis Date = 12/12/16 SpikeMix = Accu 216041125: 40 µl & Crescent 03FF058: 40 µl Pct Recovery = 100% Analysis Date = 07/20/16 SpikeMix = Supelco LC20141V: 40 µl & Accu 216041125: 40 µl Pct Recovery = 94% Analysis Date = 08/12/16 SpikeMix = ChemService 5082900: 25 µl & Phenova B20160319: 25 µl Pct Recovery = 96% Analysis Date = 06/21/16 SpikeMix = Phenova B20160319: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 96% Analysis Date = 09/08/16 SpikeMix = Supelco LC20141V: 25 µl & Accu 216041125: 25 µl Pct Recovery = 87% Analysis Date = 05/24/16 SpikeMix = Accu 216041125: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 98% Analysis Date = 03/19/15 SpikeMix = Spex Organics C1140417015: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 131% Analysis Date = 03/06/15 SpikeMix = ERA 0227-14-06.1A: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 97% Analysis Date = 12/17/14 SpikeMix = Supelco LC06438: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 95% Analysis Date = 11/22/14 SpikeMix = NSI 032614: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 127% Analysis Date = 09/21/14 SpikeMix = Supelco LC06438: 20 µl Pct Recovery = 93% Analysis Date = 08/19/14 SpikeMix = Spex Organics C1140417015: 20 µl & Accu 214031115: 20 µl Pct Recovery = 128% Analysis Date = 08/16/14 SpikeMix = ERA 0227-14-06.1A: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 128% Analysis Date = 06/10/14 SpikeMix = NSI 032614: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 103% Analysis Date = 09/29/15 SpikeMix = Accu 215041380: 25 µl & ERA 0406-15-03: 25 µl Pct Recovery = 105% Analysis Date = 08/15/15 SpikeMix = Supelco LC13545: 25 µl & Crescent 04EE008: 25 µl Pct Recovery = 110% Analysis Date = 07/13/15 SpikeMix = Crescent 04EE008: 25 µl & NSI 050515AVOC: 25 µl Pct Recovery = 108% Analysis Date = 11/29/16 SpikeMix = ChemService 5082900: 15 µl & Phenova B20160319: 15 µl Pct Recovery = 93% Analysis Date = 09/08/16 SpikeMix = Phenova B20160319: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 99% Analysis Date = 05/27/16 SpikeMix = Phenova B20160319: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 93% Analysis Date = 08/20/16 SpikeMix = Accu 216041125: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 105% Analysis Date = 06/30/16 SpikeMix = ChemService 5082900: 15 µl & Accu 216041125: 15 µl Pct Recovery = 72% Analysis Date = 04/02/16 SpikeMix = Supelco LC13545: 15 µl & Accu 215041380: 15 µl Pct Recovery = 111% Analysis Date = 03/04/16 SpikeMix = Accu 215041380: 15 µl & ERA 0406-15-03: 15 µl Pct Recovery = 95% Analysis Date = 06/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Accu 215041380: 15 µl Pct Recovery = 98% Analysis Date = 12/18/15 SpikeMix = Supelco LC13545: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 97% Analysis Date = 10/17/15 SpikeMix = Crescent 04EE008: 15 µl & NSI 050515AVOC: 15 µl Pct Recovery = 97% Analysis Date = 05/09/15 SpikeMix = Spex Organics EN150428007: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 107% Analysis Date = 11/06/14 SpikeMix = Spex Organics C1140417015: 10 µl & Crescent 03DD004: 10 µl Pct Recovery = 129% Analysis Date = 10/21/14 SpikeMix = ERA 0227-14-06.1A: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 97% Analysis Date = 09/09/14 SpikeMix = NSI 032614: 10 µl & Spex Organics C1140417015: 10 µl Pct Recovery = 128% Analysis Date = 07/23/14 SpikeMix = Spex Organics C1140417015: 10 µl & Accu 214031115: 10 µl Pct Recovery = 137% Analysis Date = 07/11/14 SpikeMix = Spex Organics C1140417015: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 125% Analysis Date = 06/18/14 SpikeMix = Supelco LC06438: 10 µl & Accu 214031115: 10 µl Pct Recovery = 111% Analysis Date = 05/30/14 SpikeMix = NSI 032614: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 99% Analysis Date = 05/03/14 SpikeMix = Crescent 03DD004: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 107% Analysis Date = 02/18/16 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 96% Analysis Date = 11/20/15 SpikeMix = Accu 215041380: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 100% Analysis Date = 11/12/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 107% Analysis Date = 05/21/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 105% Analysis Date = 05/13/16 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 110% Analysis Date = 01/27/16 SpikeMix = Crescent 04EE008: 10 µl & NSI 050515AVOC: 10 µl Pct Recovery = 113% Analysis Date = 07/31/15 SpikeMix = Crescent 04EE008: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 97% Analysis Date = 05/09/15 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 103% Analysis Date = 12/12/16 Pct Recovery = 93% Analysis Date = 12/07/16 Pct Recovery = 93% Analysis Date = 12/07/16 Pct Recovery = 93% Analysis Date = 12/02/16 Pct Recovery = 93% Analysis Date = 12/02/16 Pct Recovery = 93% Analysis Date = 11/27/16 Pct Recovery = 94% Analysis Date = 11/27/16 Pct Recovery = 94% Analysis Date = 11/22/16 Pct Recovery = 94% Analysis Date = 11/22/16 Pct Recovery = 94% Analysis Date = 11/18/16 Pct Recovery = 94% Analysis Date = 11/18/16 Pct Recovery = 94% Analysis Date = 11/13/16 Pct Recovery = 94% Analysis Date = 11/13/16 Pct Recovery = 94% Analysis Date = 11/08/16 Pct Recovery = 94% Analysis Date = 11/08/16 Pct Recovery = 94% Analysis Date = 11/03/16 Pct Recovery = 94% Analysis Date = 11/03/16 Pct Recovery = 94% Analysis Date = 10/30/16 Pct Recovery = 94% Analysis Date = 10/30/16 Pct Recovery = 94% Analysis Date = 10/25/16 Pct Recovery = 94% Analysis Date = 10/25/16 Pct Recovery = 94% Analysis Date = 10/20/16 Pct Recovery = 94% Analysis Date = 10/20/16 Pct Recovery = 94% Analysis Date = 10/15/16 Pct Recovery = 94% Analysis Date = 10/15/16 Pct Recovery = 94% Analysis Date = 10/10/16 Pct Recovery = 95% Analysis Date = 10/10/16 Pct Recovery = 95% Analysis Date = 10/06/16 Pct Recovery = 95% Analysis Date = 10/06/16 Pct Recovery = 95% Analysis Date = 10/01/16 Pct Recovery = 95% Analysis Date = 10/01/16 Pct Recovery = 95% Analysis Date = 09/26/16 Pct Recovery = 95% Analysis Date = 09/26/16 Pct Recovery = 95% Analysis Date = 09/21/16 Pct Recovery = 95% Analysis Date = 09/21/16 Pct Recovery = 95% Analysis Date = 09/17/16 Pct Recovery = 95% Analysis Date = 09/17/16 Pct Recovery = 95% Analysis Date = 09/12/16 Pct Recovery = 95% Analysis Date = 09/12/16 Pct Recovery = 95% Analysis Date = 09/07/16 Pct Recovery = 95% Analysis Date = 09/07/16 Pct Recovery = 95% Analysis Date = 09/02/16 Pct Recovery = 95% Analysis Date = 09/02/16 Pct Recovery = 95% Analysis Date = 08/29/16 Pct Recovery = 96% Analysis Date = 08/29/16 Pct Recovery = 96% Analysis Date = 08/24/16 Pct Recovery = 96% Analysis Date = 08/24/16 Pct Recovery = 96% Analysis Date = 08/19/16 Pct Recovery = 96% Analysis Date = 08/19/16 Pct Recovery = 96% Analysis Date = 08/14/16 Pct Recovery = 96% Analysis Date = 08/14/16 Pct Recovery = 96% Analysis Date = 08/09/16 Pct Recovery = 96% Analysis Date = 08/09/16 Pct Recovery = 96% Analysis Date = 08/05/16 Pct Recovery = 96% Analysis Date = 08/05/16 Pct Recovery = 96% Analysis Date = 07/31/16 Pct Recovery = 96% Analysis Date = 07/31/16 Pct Recovery = 96% Analysis Date = 07/26/16 Pct Recovery = 96% Analysis Date = 07/26/16 Pct Recovery = 96% Analysis Date = 07/21/16 Pct Recovery = 96% Analysis Date = 07/21/16 Pct Recovery = 96% Analysis Date = 07/17/16 Pct Recovery = 96% Analysis Date = 07/17/16 Pct Recovery = 96% Analysis Date = 07/12/16 Pct Recovery = 97% Analysis Date = 07/12/16 Pct Recovery = 97% Analysis Date = 07/07/16 Pct Recovery = 97% Analysis Date = 07/07/16 Pct Recovery = 97% Analysis Date = 07/02/16 Pct Recovery = 97% Analysis Date = 07/02/16 Pct Recovery = 97% Analysis Date = 06/28/16 Pct Recovery = 97% Analysis Date = 06/28/16 Pct Recovery = 97% Analysis Date = 06/23/16 Pct Recovery = 97% Analysis Date = 06/23/16 Pct Recovery = 97% Analysis Date = 06/18/16 Pct Recovery = 97% Analysis Date = 06/18/16 Pct Recovery = 97% Analysis Date = 06/13/16 Pct Recovery = 97% Analysis Date = 06/13/16 Pct Recovery = 97% Analysis Date = 06/08/16 Pct Recovery = 97% Analysis Date = 06/08/16 Pct Recovery = 97% Analysis Date = 06/04/16 Pct Recovery = 97% Analysis Date = 06/04/16 Pct Recovery = 97% Analysis Date = 05/30/16 Pct Recovery = 98% Analysis Date = 05/30/16 Pct Recovery = 98% Analysis Date = 05/25/16 Pct Recovery = 98% Analysis Date = 05/25/16 Pct Recovery = 98% Analysis Date = 05/20/16 Pct Recovery = 98% Analysis Date = 05/20/16 Pct Recovery = 98% Analysis Date = 05/16/16 Pct Recovery = 98% Analysis Date = 05/16/16 Pct Recovery = 98% Analysis Date = 05/11/16 Pct Recovery = 98% Analysis Date = 05/11/16 Pct Recovery = 98% Analysis Date = 05/06/16 Pct Recovery = 98% Analysis Date = 05/06/16 Pct Recovery = 98% Analysis Date = 05/01/16 Pct Recovery = 98% Analysis Date = 05/01/16 Pct Recovery = 98% Analysis Date = 04/27/16 Pct Recovery = 98% Analysis Date = 04/27/16 Pct Recovery = 98% Analysis Date = 04/22/16 Pct Recovery = 98% Analysis Date = 04/22/16 Pct Recovery = 98% Analysis Date = 04/17/16 Pct Recovery = 99% Analysis Date = 04/17/16 Pct Recovery = 99% Analysis Date = 04/12/16 Pct Recovery = 99% Analysis Date = 04/12/16 Pct Recovery = 99% Analysis Date = 04/07/16 Pct Recovery = 99% Analysis Date = 04/07/16 Pct Recovery = 99% Analysis Date = 04/03/16 Pct Recovery = 99% Analysis Date = 04/03/16 Pct Recovery = 99% Analysis Date = 03/29/16 Pct Recovery = 99% Analysis Date = 03/29/16 Pct Recovery = 99% Analysis Date = 03/24/16 Pct Recovery = 99% Analysis Date = 03/24/16 Pct Recovery = 99% Analysis Date = 03/19/16 Pct Recovery = 99% Analysis Date = 03/19/16 Pct Recovery = 99% Analysis Date = 03/15/16 Pct Recovery = 99% Analysis Date = 03/15/16 Pct Recovery = 99% Analysis Date = 03/10/16 Pct Recovery = 100% Analysis Date = 03/10/16 Pct Recovery = 100% Analysis Date = 03/05/16 Pct Recovery = 100% Analysis Date = 03/05/16 Pct Recovery = 100% Analysis Date = 02/29/16 Pct Recovery = 100% Analysis Date = 02/29/16 Pct Recovery = 100% Analysis Date = 02/25/16 Pct Recovery = 100% Analysis Date = 02/25/16 Pct Recovery = 100% Analysis Date = 02/20/16 Pct Recovery = 100% Analysis Date = 02/20/16 Pct Recovery = 100% Analysis Date = 02/15/16 Pct Recovery = 100% Analysis Date = 02/15/16 Pct Recovery = 100% Analysis Date = 02/10/16 Pct Recovery = 100% Analysis Date = 02/10/16 Pct Recovery = 100% Analysis Date = 02/05/16 Pct Recovery = 100% Analysis Date = 02/05/16 Pct Recovery = 100% Analysis Date = 02/01/16 Pct Recovery = 101% Analysis Date = 02/01/16 Pct Recovery = 101% Analysis Date = 01/27/16 Pct Recovery = 101% Analysis Date = 01/27/16 Pct Recovery = 101% Analysis Date = 01/22/16 Pct Recovery = 101% Analysis Date = 01/22/16 Pct Recovery = 101% Analysis Date = 01/17/16 Pct Recovery = 101% Analysis Date = 01/17/16 Pct Recovery = 101% Analysis Date = 01/13/16 Pct Recovery = 101% Analysis Date = 01/13/16 Pct Recovery = 101% Analysis Date = 01/08/16 Pct Recovery = 101% Analysis Date = 01/08/16 Pct Recovery = 101% Analysis Date = 01/03/16 Pct Recovery = 101% Analysis Date = 01/03/16 Pct Recovery = 101% Analysis Date = 12/29/15 Pct Recovery = 101% Analysis Date = 12/29/15 Pct Recovery = 101% Analysis Date = 12/25/15 Pct Recovery = 102% Analysis Date = 12/25/15 Pct Recovery = 102% Analysis Date = 12/20/15 Pct Recovery = 102% Analysis Date = 12/20/15 Pct Recovery = 102% Analysis Date = 12/15/15 Pct Recovery = 102% Analysis Date = 12/15/15 Pct Recovery = 102% Analysis Date = 12/10/15 Pct Recovery = 102% Analysis Date = 12/10/15 Pct Recovery = 102% Analysis Date = 12/05/15 Pct Recovery = 102% Analysis Date = 12/05/15 Pct Recovery = 102% Analysis Date = 12/01/15 Pct Recovery = 102% Analysis Date = 12/01/15 Pct Recovery = 102% Analysis Date = 11/26/15 Pct Recovery = 102% Analysis Date = 11/26/15 Pct Recovery = 102% Analysis Date = 11/21/15 Pct Recovery = 102% Analysis Date = 11/21/15 Pct Recovery = 102% Analysis Date = 11/16/15 Pct Recovery = 102% Analysis Date = 11/16/15 Pct Recovery = 102% Analysis Date = 11/12/15 Pct Recovery = 102% Analysis Date = 11/12/15 Pct Recovery = 102% Analysis Date = 11/07/15 Pct Recovery = 103% Analysis Date = 11/07/15 Pct Recovery = 103% Analysis Date = 11/02/15 Pct Recovery = 103% Analysis Date = 11/02/15 Pct Recovery = 103% Analysis Date = 10/28/15 Pct Recovery = 103% Analysis Date = 10/28/15 Pct Recovery = 103% Analysis Date = 10/24/15 Pct Recovery = 103% Analysis Date = 10/24/15 Pct Recovery = 103% Analysis Date = 10/19/15 Pct Recovery = 103% Analysis Date = 10/19/15 Pct Recovery = 103% Analysis Date = 10/14/15 Pct Recovery = 103% Analysis Date = 10/14/15 Pct Recovery = 103% Analysis Date = 10/09/15 Pct Recovery = 103% Analysis Date = 10/09/15 Pct Recovery = 103% Analysis Date = 10/04/15 Pct Recovery = 103% Analysis Date = 10/04/15 Pct Recovery = 103% Analysis Date = 09/30/15 Pct Recovery = 103% Analysis Date = 09/30/15 Pct Recovery = 103% Analysis Date = 09/25/15 Pct Recovery = 103% Analysis Date = 09/25/15 Pct Recovery = 103% Analysis Date = 09/20/15 Pct Recovery = 103% Analysis Date = 09/20/15 Pct Recovery = 103% Analysis Date = 09/15/15 Pct Recovery = 104% Analysis Date = 09/15/15 Pct Recovery = 104% Analysis Date = 09/11/15 Pct Recovery = 104% Analysis Date = 09/11/15 Pct Recovery = 104% Analysis Date = 09/06/15 Pct Recovery = 104% Analysis Date = 09/06/15 Pct Recovery = 104% Analysis Date = 09/01/15 Pct Recovery = 104% Analysis Date = 09/01/15 Pct Recovery = 104% Analysis Date = 08/27/15 Pct Recovery = 104% Analysis Date = 08/27/15 Pct Recovery = 104% Analysis Date = 08/23/15 Pct Recovery = 104% Analysis Date = 08/23/15 Pct Recovery = 104% Analysis Date = 08/18/15 Pct Recovery = 104% Analysis Date = 08/18/15 Pct Recovery = 104% Analysis Date = 08/13/15 Pct Recovery = 104% Analysis Date = 08/13/15 Pct Recovery = 104% Analysis Date = 08/08/15 Pct Recovery = 104% Analysis Date = 08/08/15 Pct Recovery = 104% Analysis Date = 08/03/15 Pct Recovery = 104% Analysis Date = 08/03/15 Pct Recovery = 104% Analysis Date = 07/30/15 Pct Recovery = 104% Analysis Date = 07/30/15 Pct Recovery = 104% Analysis Date = 07/25/15 Pct Recovery = 105% Analysis Date = 07/25/15 Pct Recovery = 105% Analysis Date = 07/20/15 Pct Recovery = 105% Analysis Date = 07/20/15 Pct Recovery = 105% Analysis Date = 07/15/15 Pct Recovery = 105% Analysis Date = 07/15/15 Pct Recovery = 105% Analysis Date = 07/11/15 Pct Recovery = 105% Analysis Date = 07/11/15 Pct Recovery = 105% Analysis Date = 07/06/15 Pct Recovery = 105% Analysis Date = 07/06/15 Pct Recovery = 105% Analysis Date = 07/01/15 Pct Recovery = 105% Analysis Date = 07/01/15 Pct Recovery = 105% Analysis Date = 06/26/15 Pct Recovery = 105% Analysis Date = 06/26/15 Pct Recovery = 105% Analysis Date = 06/21/15 Pct Recovery = 105% Analysis Date = 06/21/15 Pct Recovery = 105% Analysis Date = 06/17/15 Pct Recovery = 106% Analysis Date = 06/17/15 Pct Recovery = 106% Analysis Date = 06/12/15 Pct Recovery = 106% Analysis Date = 06/12/15 Pct Recovery = 106% Analysis Date = 06/07/15 Pct Recovery = 106% Analysis Date = 06/07/15 Pct Recovery = 106% Analysis Date = 06/02/15 Pct Recovery = 106% Analysis Date = 06/02/15 Pct Recovery = 106% Analysis Date = 05/29/15 Pct Recovery = 106% Analysis Date = 05/29/15 Pct Recovery = 106% Analysis Date = 05/24/15 Pct Recovery = 106% Analysis Date = 05/24/15 Pct Recovery = 106% Analysis Date = 05/19/15 Pct Recovery = 106% Analysis Date = 05/19/15 Pct Recovery = 106% Analysis Date = 05/14/15 Pct Recovery = 106% Analysis Date = 05/14/15 Pct Recovery = 106% Analysis Date = 05/10/15 Pct Recovery = 106% Analysis Date = 05/10/15 Pct Recovery = 106% Analysis Date = 05/05/15 Pct Recovery = 107% Analysis Date = 05/05/15 Pct Recovery = 107% Analysis Date = 04/30/15 Pct Recovery = 107% Analysis Date = 04/30/15 Pct Recovery = 107% Analysis Date = 04/25/15 Pct Recovery = 107% Analysis Date = 04/25/15 Pct Recovery = 107% Analysis Date = 04/20/15 Pct Recovery = 107% Analysis Date = 04/20/15 Pct Recovery = 107% Analysis Date = 04/16/15 Pct Recovery = 107% Analysis Date = 04/16/15 Pct Recovery = 107% Analysis Date = 04/11/15 Pct Recovery = 108% Analysis Date = 04/11/15 Pct Recovery = 108% Analysis Date = 04/06/15 Pct Recovery = 108% Analysis Date = 04/06/15 Pct Recovery = 108% Analysis Date = 04/01/15 Pct Recovery = 108% Analysis Date = 04/01/15 Pct Recovery = 108% Analysis Date = 03/28/15 Pct Recovery = 108% Analysis Date = 03/28/15 Pct Recovery = 108% Analysis Date = 03/23/15 Pct Recovery = 108% Analysis Date = 03/23/15 Pct Recovery = 108% Analysis Date = 03/18/15 Pct Recovery = 108% Analysis Date = 03/18/15 Pct Recovery = 108% Analysis Date = 03/13/15 Pct Recovery = 109% Analysis Date = 03/13/15 Pct Recovery = 109% Analysis Date = 03/09/15 Pct Recovery = 109% Analysis Date = 03/09/15 Pct Recovery = 109% Analysis Date = 03/04/15 Pct Recovery = 109% Analysis Date = 03/04/15 Pct Recovery = 109% Analysis Date = 02/27/15 Pct Recovery = 109% Analysis Date = 02/27/15 Pct Recovery = 109% Analysis Date = 02/22/15 Pct Recovery = 109% Analysis Date = 02/22/15 Pct Recovery = 109% Analysis Date = 02/17/15 Pct Recovery = 110% Analysis Date = 02/17/15 Pct Recovery = 110% Analysis Date = 02/13/15 Pct Recovery = 110% Analysis Date = 02/13/15 Pct Recovery = 110% Analysis Date = 02/08/15 Pct Recovery = 110% Analysis Date = 02/08/15 Pct Recovery = 110% Analysis Date = 02/03/15 Pct Recovery = 110% Analysis Date = 02/03/15 Pct Recovery = 110% Analysis Date = 01/29/15 Pct Recovery = 110% Analysis Date = 01/29/15 Pct Recovery = 110% Analysis Date = 01/25/15 Pct Recovery = 110% Analysis Date = 01/25/15 Pct Recovery = 110% Analysis Date = 01/20/15 Pct Recovery = 111% Analysis Date = 01/20/15 Pct Recovery = 111% Analysis Date = 01/15/15 Pct Recovery = 111% Analysis Date = 01/15/15 Pct Recovery = 111% Analysis Date = 01/10/15 Pct Recovery = 111% Analysis Date = 01/10/15 Pct Recovery = 111% Analysis Date = 01/06/15 Pct Recovery = 111% Analysis Date = 01/06/15 Pct Recovery = 111% Analysis Date = 01/01/15 Pct Recovery = 111% Analysis Date = 01/01/15 Pct Recovery = 111% Analysis Date = 12/27/14 Pct Recovery = 111% Analysis Date = 12/27/14 Pct Recovery = 111% Analysis Date = 12/22/14 Pct Recovery = 112% Analysis Date = 12/22/14 Pct Recovery = 112% Analysis Date = 12/17/14 Pct Recovery = 112% Analysis Date = 12/17/14 Pct Recovery = 112% Analysis Date = 12/13/14 Pct Recovery = 112% Analysis Date = 12/13/14 Pct Recovery = 112% Analysis Date = 12/08/14 Pct Recovery = 112% Analysis Date = 12/08/14 Pct Recovery = 112% Analysis Date = 12/03/14 Pct Recovery = 112% Analysis Date = 12/03/14 Pct Recovery = 112% Analysis Date = 11/28/14 Pct Recovery = 112% Analysis Date = 11/28/14 Pct Recovery = 112% Analysis Date = 11/24/14 Pct Recovery = 112% Analysis Date = 11/24/14 Pct Recovery = 112% Analysis Date = 11/19/14 Pct Recovery = 112% Analysis Date = 11/19/14 Pct Recovery = 112% Analysis Date = 11/14/14 Pct Recovery = 113% Analysis Date = 11/14/14 Pct Recovery = 113% Analysis Date = 11/09/14 Pct Recovery = 113% Analysis Date = 11/09/14 Pct Recovery = 113% Analysis Date = 11/05/14 Pct Recovery = 113% Analysis Date = 11/05/14 Pct Recovery = 113% Analysis Date = 10/31/14 Pct Recovery = 113% Analysis Date = 10/31/14 Pct Recovery = 113% Analysis Date = 10/26/14 Pct Recovery = 113% Analysis Date = 10/26/14 Pct Recovery = 113% Analysis Date = 10/21/14 Pct Recovery = 113% Analysis Date = 10/21/14 Pct Recovery = 113% Analysis Date = 10/16/14 Pct Recovery = 113% Analysis Date = 10/16/14 Pct Recovery = 113% Analysis Date = 10/12/14 Pct Recovery = 113% Analysis Date = 10/12/14 Pct Recovery = 113% Analysis Date = 10/07/14 Pct Recovery = 113% Analysis Date = 10/07/14 Pct Recovery = 113% Analysis Date = 10/02/14 Pct Recovery = 113% Analysis Date = 10/02/14 Pct Recovery = 113% Analysis Date = 09/27/14 Pct Recovery = 113% Analysis Date = 09/27/14 Pct Recovery = 113% Analysis Date = 09/23/14 Pct Recovery = 114% Analysis Date = 09/23/14 Pct Recovery = 114% Analysis Date = 09/18/14 Pct Recovery = 114% Analysis Date = 09/18/14 Pct Recovery = 114% Analysis Date = 09/13/14 Pct Recovery = 114% Analysis Date = 09/13/14 Pct Recovery = 114% Analysis Date = 09/08/14 Pct Recovery = 114% Analysis Date = 09/08/14 Pct Recovery = 114% Analysis Date = 09/04/14 Pct Recovery = 114% Analysis Date = 09/04/14 Pct Recovery = 114% Analysis Date = 08/30/14 Pct Recovery = 114% Analysis Date = 08/30/14 Pct Recovery = 114% Analysis Date = 08/25/14 Pct Recovery = 114% Analysis Date = 08/25/14 Pct Recovery = 114% Analysis Date = 08/20/14 Pct Recovery = 114% Analysis Date = 08/20/14 Pct Recovery = 114% Analysis Date = 08/15/14 Pct Recovery = 114% Analysis Date = 08/15/14 Pct Recovery = 114% Analysis Date = 08/11/14 Pct Recovery = 114% Analysis Date = 08/11/14 Pct Recovery = 114% Analysis Date = 08/06/14 Pct Recovery = 114% Analysis Date = 08/06/14 Pct Recovery = 114% Analysis Date = 08/01/14 Pct Recovery = 115% Analysis Date = 08/01/14 Pct Recovery = 115% Analysis Date = 07/27/14 Pct Recovery = 115% Analysis Date = 07/27/14 Pct Recovery = 115% Analysis Date = 07/23/14 Pct Recovery = 115% Analysis Date = 07/23/14 Pct Recovery = 115% Analysis Date = 07/18/14 Pct Recovery = 115% Analysis Date = 07/18/14 Pct Recovery = 115% Analysis Date = 07/13/14 Pct Recovery = 115% Analysis Date = 07/13/14 Pct Recovery = 115% Analysis Date = 07/08/14 Pct Recovery = 115% Analysis Date = 07/08/14 Pct Recovery = 115% Analysis Date = 07/04/14 Pct Recovery = 115% Analysis Date = 07/04/14 Pct Recovery = 115% Analysis Date = 06/29/14 Pct Recovery = 115% Analysis Date = 06/29/14 Pct Recovery = 115% Analysis Date = 06/24/14 Pct Recovery = 115% Analysis Date = 06/24/14 Pct Recovery = 115% Analysis Date = 06/19/14 Pct Recovery = 115% Analysis Date = 06/19/14 Pct Recovery = 115% Analysis Date = 06/14/14 Pct Recovery = 115% Analysis Date = 06/14/14 Pct Recovery = 115% Analysis Date = 06/10/14 Pct Recovery = 115% Analysis Date = 06/10/14 Pct Recovery = 115% Analysis Date = 06/05/14 Pct Recovery = 115% Analysis Date = 06/05/14 Pct Recovery = 115% Analysis Date = 05/31/14 Pct Recovery = 116% Analysis Date = 05/31/14 Pct Recovery = 116% Analysis Date = 05/26/14 Pct Recovery = 116% Analysis Date = 05/26/14 Pct Recovery = 116% Analysis Date = 05/22/14 Pct Recovery = 116% Analysis Date = 05/22/14 Pct Recovery = 116% Analysis Date = 05/17/14 Pct Recovery = 116% Analysis Date = 05/17/14 Pct Recovery = 116% Analysis Date = 05/12/14 Pct Recovery = 116% Analysis Date = 05/12/14 Pct Recovery = 116% Analysis Date = 05/07/14 Pct Recovery = 116% Analysis Date = 05/07/14 Pct Recovery = 116% Analysis Date = 05/03/14 Pct Recovery = 116% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
CHLOROFORM

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 44 105% 13% 101% 10%
Total 44 105% 13% 101% 10%

Sample Statistics
CHLOROFORM

Characteristic N % % Basis
Plotted 44 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 44 .  
False Negatives 0 0% 0 out of 44
Not Spiked 22 .  
False Positives 0 0% 0 out of 22

BQS OBSP Determination:
CHLOROMETHANE
METHOD: 4440 , TESTIDCODE: 34418GCM66
Open Data Set

Analysis Date = 07/23/14 SpikeMix = Spex Organics C1140417015: 10 µl & Accu 214031115: 10 µl Pct Recovery = 200% Analysis Date = 12/12/16 SpikeMix = Accu 216041125: 40 µl & Crescent 03FF058: 40 µl Pct Recovery = 75% Analysis Date = 07/20/16 SpikeMix = Supelco LC20141V: 40 µl & Accu 216041125: 40 µl Pct Recovery = 121% Analysis Date = 07/14/16 SpikeMix = Accu 216041125: 40 µl & NSI 041816AVOC: 40 µl Pct Recovery = 106% Analysis Date = 08/12/16 SpikeMix = ChemService 5082900: 25 µl & Phenova B20160319: 25 µl Pct Recovery = 120% Analysis Date = 06/21/16 SpikeMix = Phenova B20160319: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 120% Analysis Date = 09/08/16 SpikeMix = Supelco LC20141V: 25 µl & Accu 216041125: 25 µl Pct Recovery = 97% Analysis Date = 05/24/16 SpikeMix = Accu 216041125: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 97% Analysis Date = 03/19/15 SpikeMix = Spex Organics C1140417015: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 125% Analysis Date = 12/17/14 SpikeMix = Supelco LC06438: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 100% Analysis Date = 11/14/14 SpikeMix = Crescent 03DD004: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 50% Analysis Date = 06/10/14 SpikeMix = Crescent 03DD004: 20 µl & NSI 032614: 20 µl Pct Recovery = 100% Analysis Date = 04/09/15 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 125% Analysis Date = 08/19/14 SpikeMix = Spex Organics C1140417015: 20 µl & Accu 214031115: 20 µl Pct Recovery = 125% Analysis Date = 07/01/14 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 75% Analysis Date = 05/01/14 SpikeMix = Accu 214031115: 20 µl & NSI 032614: 20 µl Pct Recovery = 75% Analysis Date = 09/29/15 SpikeMix = Accu 215041380: 25 µl & ERA 0406-15-03: 25 µl Pct Recovery = 107% Analysis Date = 07/13/15 SpikeMix = Crescent 04EE008: 25 µl & NSI 050515AVOC: 25 µl Pct Recovery = 107% Analysis Date = 06/16/15 SpikeMix = ERA 0406-15-03: 25 µl & Supelco LC13545: 25 µl Pct Recovery = 80% Analysis Date = 11/29/16 SpikeMix = ChemService 5082900: 15 µl & Phenova B20160319: 15 µl Pct Recovery = 80% Analysis Date = 09/08/16 SpikeMix = Phenova B20160319: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 80% Analysis Date = 07/29/16 SpikeMix = Phenova B20160319: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 120% Analysis Date = 05/27/16 SpikeMix = Phenova B20160319: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 80% Analysis Date = 10/13/16 SpikeMix = Accu 216041125: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 121% Analysis Date = 08/20/16 SpikeMix = Accu 216041125: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 121% Analysis Date = 07/06/16 SpikeMix = ChemService 5082900: 15 µl & Accu 216041125: 15 µl Pct Recovery = 121% Analysis Date = 04/26/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 89% Analysis Date = 03/04/16 SpikeMix = Accu 215041380: 15 µl & ERA 0406-15-03: 15 µl Pct Recovery = 89% Analysis Date = 02/05/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 133% Analysis Date = 11/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 89% Analysis Date = 10/17/15 SpikeMix = Crescent 04EE008: 15 µl & NSI 050515AVOC: 15 µl Pct Recovery = 133% Analysis Date = 10/16/15 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 178% Analysis Date = 06/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Accu 215041380: 15 µl Pct Recovery = 89% Analysis Date = 11/06/14 SpikeMix = Spex Organics C1140417015: 10 µl & Crescent 03DD004: 10 µl Pct Recovery = 100% Analysis Date = 10/04/14 SpikeMix = Crescent 03DD004: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 100% Analysis Date = 07/29/14 SpikeMix = Crescent 03DD004: 10 µl & NSI 032614: 10 µl Pct Recovery = 100% Analysis Date = 05/03/14 SpikeMix = Crescent 03DD004: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 100% Analysis Date = 01/13/15 SpikeMix = Accu 214031115: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 100% Analysis Date = 09/09/14 SpikeMix = Accu 214031115: 10 µl & NSI 032614: 10 µl Pct Recovery = 150% Analysis Date = 07/23/14 SpikeMix = Spex Organics C1140417015: 10 µl & Accu 214031115: 10 µl Pct Recovery = 200% Analysis Date = 06/18/14 SpikeMix = Supelco LC06438: 10 µl & Accu 214031115: 10 µl Pct Recovery = 100% Analysis Date = 03/17/16 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 67% Analysis Date = 01/27/16 SpikeMix = Crescent 04EE008: 10 µl & NSI 050515AVOC: 10 µl Pct Recovery = 133% Analysis Date = 12/10/15 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 67% Analysis Date = 11/20/15 SpikeMix = Accu 215041380: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 133% Analysis Date = 09/03/15 SpikeMix = NSI 050515AVOC: 10 µl & Spex Organics EN150428007: 10 µl Pct Recovery = 133% Analysis Date = 07/31/15 SpikeMix = Crescent 04EE008: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 133% Analysis Date = 06/27/15 SpikeMix = ERA 0406-15-03: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 200% Analysis Date = 12/11/16 Pct Recovery = 97% Analysis Date = 12/07/16 Pct Recovery = 97% Analysis Date = 12/07/16 Pct Recovery = 97% Analysis Date = 12/02/16 Pct Recovery = 97% Analysis Date = 12/02/16 Pct Recovery = 97% Analysis Date = 11/27/16 Pct Recovery = 97% Analysis Date = 11/27/16 Pct Recovery = 97% Analysis Date = 11/22/16 Pct Recovery = 98% Analysis Date = 11/22/16 Pct Recovery = 98% Analysis Date = 11/18/16 Pct Recovery = 98% Analysis Date = 11/18/16 Pct Recovery = 98% Analysis Date = 11/13/16 Pct Recovery = 98% Analysis Date = 11/13/16 Pct Recovery = 98% Analysis Date = 11/08/16 Pct Recovery = 98% Analysis Date = 11/08/16 Pct Recovery = 98% Analysis Date = 11/03/16 Pct Recovery = 98% Analysis Date = 11/03/16 Pct Recovery = 98% Analysis Date = 10/29/16 Pct Recovery = 99% Analysis Date = 10/29/16 Pct Recovery = 99% Analysis Date = 10/25/16 Pct Recovery = 99% Analysis Date = 10/25/16 Pct Recovery = 99% Analysis Date = 10/20/16 Pct Recovery = 99% Analysis Date = 10/20/16 Pct Recovery = 99% Analysis Date = 10/15/16 Pct Recovery = 99% Analysis Date = 10/15/16 Pct Recovery = 99% Analysis Date = 10/10/16 Pct Recovery = 99% Analysis Date = 10/10/16 Pct Recovery = 99% Analysis Date = 10/06/16 Pct Recovery = 100% Analysis Date = 10/06/16 Pct Recovery = 100% Analysis Date = 10/01/16 Pct Recovery = 100% Analysis Date = 10/01/16 Pct Recovery = 100% Analysis Date = 09/26/16 Pct Recovery = 100% Analysis Date = 09/26/16 Pct Recovery = 100% Analysis Date = 09/21/16 Pct Recovery = 100% Analysis Date = 09/21/16 Pct Recovery = 100% Analysis Date = 09/16/16 Pct Recovery = 100% Analysis Date = 09/16/16 Pct Recovery = 100% Analysis Date = 09/12/16 Pct Recovery = 101% Analysis Date = 09/12/16 Pct Recovery = 101% Analysis Date = 09/07/16 Pct Recovery = 101% Analysis Date = 09/07/16 Pct Recovery = 101% Analysis Date = 09/02/16 Pct Recovery = 101% Analysis Date = 09/02/16 Pct Recovery = 101% Analysis Date = 08/28/16 Pct Recovery = 101% Analysis Date = 08/28/16 Pct Recovery = 101% Analysis Date = 08/24/16 Pct Recovery = 101% Analysis Date = 08/24/16 Pct Recovery = 101% Analysis Date = 08/19/16 Pct Recovery = 102% Analysis Date = 08/19/16 Pct Recovery = 102% Analysis Date = 08/14/16 Pct Recovery = 102% Analysis Date = 08/14/16 Pct Recovery = 102% Analysis Date = 08/09/16 Pct Recovery = 102% Analysis Date = 08/09/16 Pct Recovery = 102% Analysis Date = 08/04/16 Pct Recovery = 102% Analysis Date = 08/04/16 Pct Recovery = 102% Analysis Date = 07/31/16 Pct Recovery = 102% Analysis Date = 07/31/16 Pct Recovery = 102% Analysis Date = 07/26/16 Pct Recovery = 103% Analysis Date = 07/26/16 Pct Recovery = 103% Analysis Date = 07/21/16 Pct Recovery = 103% Analysis Date = 07/21/16 Pct Recovery = 103% Analysis Date = 07/16/16 Pct Recovery = 103% Analysis Date = 07/16/16 Pct Recovery = 103% Analysis Date = 07/12/16 Pct Recovery = 103% Analysis Date = 07/12/16 Pct Recovery = 103% Analysis Date = 07/07/16 Pct Recovery = 103% Analysis Date = 07/07/16 Pct Recovery = 103% Analysis Date = 07/02/16 Pct Recovery = 104% Analysis Date = 07/02/16 Pct Recovery = 104% Analysis Date = 06/27/16 Pct Recovery = 104% Analysis Date = 06/27/16 Pct Recovery = 104% Analysis Date = 06/22/16 Pct Recovery = 104% Analysis Date = 06/22/16 Pct Recovery = 104% Analysis Date = 06/18/16 Pct Recovery = 104% Analysis Date = 06/18/16 Pct Recovery = 104% Analysis Date = 06/13/16 Pct Recovery = 105% Analysis Date = 06/13/16 Pct Recovery = 105% Analysis Date = 06/08/16 Pct Recovery = 105% Analysis Date = 06/08/16 Pct Recovery = 105% Analysis Date = 06/03/16 Pct Recovery = 105% Analysis Date = 06/03/16 Pct Recovery = 105% Analysis Date = 05/30/16 Pct Recovery = 105% Analysis Date = 05/30/16 Pct Recovery = 105% Analysis Date = 05/25/16 Pct Recovery = 105% Analysis Date = 05/25/16 Pct Recovery = 105% Analysis Date = 05/20/16 Pct Recovery = 106% Analysis Date = 05/20/16 Pct Recovery = 106% Analysis Date = 05/15/16 Pct Recovery = 106% Analysis Date = 05/15/16 Pct Recovery = 106% Analysis Date = 05/10/16 Pct Recovery = 106% Analysis Date = 05/10/16 Pct Recovery = 106% Analysis Date = 05/06/16 Pct Recovery = 106% Analysis Date = 05/06/16 Pct Recovery = 106% Analysis Date = 05/01/16 Pct Recovery = 107% Analysis Date = 05/01/16 Pct Recovery = 107% Analysis Date = 04/26/16 Pct Recovery = 107% Analysis Date = 04/26/16 Pct Recovery = 107% Analysis Date = 04/21/16 Pct Recovery = 107% Analysis Date = 04/21/16 Pct Recovery = 107% Analysis Date = 04/16/16 Pct Recovery = 107% Analysis Date = 04/16/16 Pct Recovery = 107% Analysis Date = 04/12/16 Pct Recovery = 107% Analysis Date = 04/12/16 Pct Recovery = 107% Analysis Date = 04/07/16 Pct Recovery = 108% Analysis Date = 04/07/16 Pct Recovery = 108% Analysis Date = 04/02/16 Pct Recovery = 108% Analysis Date = 04/02/16 Pct Recovery = 108% Analysis Date = 03/28/16 Pct Recovery = 108% Analysis Date = 03/28/16 Pct Recovery = 108% Analysis Date = 03/24/16 Pct Recovery = 108% Analysis Date = 03/24/16 Pct Recovery = 108% Analysis Date = 03/19/16 Pct Recovery = 108% Analysis Date = 03/19/16 Pct Recovery = 108% Analysis Date = 03/14/16 Pct Recovery = 108% Analysis Date = 03/14/16 Pct Recovery = 108% Analysis Date = 03/09/16 Pct Recovery = 109% Analysis Date = 03/09/16 Pct Recovery = 109% Analysis Date = 03/04/16 Pct Recovery = 109% Analysis Date = 03/04/16 Pct Recovery = 109% Analysis Date = 02/29/16 Pct Recovery = 109% Analysis Date = 02/29/16 Pct Recovery = 109% Analysis Date = 02/24/16 Pct Recovery = 109% Analysis Date = 02/24/16 Pct Recovery = 109% Analysis Date = 02/19/16 Pct Recovery = 109% Analysis Date = 02/19/16 Pct Recovery = 109% Analysis Date = 02/14/16 Pct Recovery = 110% Analysis Date = 02/14/16 Pct Recovery = 110% Analysis Date = 02/10/16 Pct Recovery = 110% Analysis Date = 02/10/16 Pct Recovery = 110% Analysis Date = 02/05/16 Pct Recovery = 110% Analysis Date = 02/05/16 Pct Recovery = 110% Analysis Date = 01/31/16 Pct Recovery = 110% Analysis Date = 01/31/16 Pct Recovery = 110% Analysis Date = 01/26/16 Pct Recovery = 111% Analysis Date = 01/26/16 Pct Recovery = 111% Analysis Date = 01/21/16 Pct Recovery = 111% Analysis Date = 01/21/16 Pct Recovery = 111% Analysis Date = 01/17/16 Pct Recovery = 111% Analysis Date = 01/17/16 Pct Recovery = 111% Analysis Date = 01/12/16 Pct Recovery = 112% Analysis Date = 01/12/16 Pct Recovery = 112% Analysis Date = 01/07/16 Pct Recovery = 112% Analysis Date = 01/07/16 Pct Recovery = 112% Analysis Date = 01/02/16 Pct Recovery = 112% Analysis Date = 01/02/16 Pct Recovery = 112% Analysis Date = 12/29/15 Pct Recovery = 113% Analysis Date = 12/29/15 Pct Recovery = 113% Analysis Date = 12/24/15 Pct Recovery = 113% Analysis Date = 12/24/15 Pct Recovery = 113% Analysis Date = 12/19/15 Pct Recovery = 113% Analysis Date = 12/19/15 Pct Recovery = 113% Analysis Date = 12/14/15 Pct Recovery = 114% Analysis Date = 12/14/15 Pct Recovery = 114% Analysis Date = 12/09/15 Pct Recovery = 114% Analysis Date = 12/09/15 Pct Recovery = 114% Analysis Date = 12/05/15 Pct Recovery = 114% Analysis Date = 12/05/15 Pct Recovery = 114% Analysis Date = 11/30/15 Pct Recovery = 115% Analysis Date = 11/30/15 Pct Recovery = 115% Analysis Date = 11/25/15 Pct Recovery = 115% Analysis Date = 11/25/15 Pct Recovery = 115% Analysis Date = 11/20/15 Pct Recovery = 115% Analysis Date = 11/20/15 Pct Recovery = 115% Analysis Date = 11/16/15 Pct Recovery = 116% Analysis Date = 11/16/15 Pct Recovery = 116% Analysis Date = 11/11/15 Pct Recovery = 116% Analysis Date = 11/11/15 Pct Recovery = 116% Analysis Date = 11/06/15 Pct Recovery = 116% Analysis Date = 11/06/15 Pct Recovery = 116% Analysis Date = 11/01/15 Pct Recovery = 116% Analysis Date = 11/01/15 Pct Recovery = 116% Analysis Date = 10/27/15 Pct Recovery = 117% Analysis Date = 10/27/15 Pct Recovery = 117% Analysis Date = 10/23/15 Pct Recovery = 117% Analysis Date = 10/23/15 Pct Recovery = 117% Analysis Date = 10/18/15 Pct Recovery = 117% Analysis Date = 10/18/15 Pct Recovery = 117% Analysis Date = 10/13/15 Pct Recovery = 118% Analysis Date = 10/13/15 Pct Recovery = 118% Analysis Date = 10/08/15 Pct Recovery = 118% Analysis Date = 10/08/15 Pct Recovery = 118% Analysis Date = 10/04/15 Pct Recovery = 118% Analysis Date = 10/04/15 Pct Recovery = 118% Analysis Date = 09/29/15 Pct Recovery = 118% Analysis Date = 09/29/15 Pct Recovery = 118% Analysis Date = 09/24/15 Pct Recovery = 118% Analysis Date = 09/24/15 Pct Recovery = 118% Analysis Date = 09/19/15 Pct Recovery = 118% Analysis Date = 09/19/15 Pct Recovery = 118% Analysis Date = 09/14/15 Pct Recovery = 118% Analysis Date = 09/14/15 Pct Recovery = 118% Analysis Date = 09/10/15 Pct Recovery = 118% Analysis Date = 09/10/15 Pct Recovery = 118% Analysis Date = 09/05/15 Pct Recovery = 118% Analysis Date = 09/05/15 Pct Recovery = 118% Analysis Date = 08/31/15 Pct Recovery = 118% Analysis Date = 08/31/15 Pct Recovery = 118% Analysis Date = 08/26/15 Pct Recovery = 119% Analysis Date = 08/26/15 Pct Recovery = 119% Analysis Date = 08/21/15 Pct Recovery = 119% Analysis Date = 08/21/15 Pct Recovery = 119% Analysis Date = 08/17/15 Pct Recovery = 119% Analysis Date = 08/17/15 Pct Recovery = 119% Analysis Date = 08/12/15 Pct Recovery = 119% Analysis Date = 08/12/15 Pct Recovery = 119% Analysis Date = 08/07/15 Pct Recovery = 119% Analysis Date = 08/07/15 Pct Recovery = 119% Analysis Date = 08/02/15 Pct Recovery = 119% Analysis Date = 08/02/15 Pct Recovery = 119% Analysis Date = 07/29/15 Pct Recovery = 119% Analysis Date = 07/29/15 Pct Recovery = 119% Analysis Date = 07/24/15 Pct Recovery = 119% Analysis Date = 07/24/15 Pct Recovery = 119% Analysis Date = 07/19/15 Pct Recovery = 119% Analysis Date = 07/19/15 Pct Recovery = 119% Analysis Date = 07/14/15 Pct Recovery = 118% Analysis Date = 07/14/15 Pct Recovery = 118% Analysis Date = 07/09/15 Pct Recovery = 118% Analysis Date = 07/09/15 Pct Recovery = 118% Analysis Date = 07/05/15 Pct Recovery = 118% Analysis Date = 07/05/15 Pct Recovery = 118% Analysis Date = 06/30/15 Pct Recovery = 118% Analysis Date = 06/30/15 Pct Recovery = 118% Analysis Date = 06/25/15 Pct Recovery = 117% Analysis Date = 06/25/15 Pct Recovery = 117% Analysis Date = 06/20/15 Pct Recovery = 117% Analysis Date = 06/20/15 Pct Recovery = 117% Analysis Date = 06/16/15 Pct Recovery = 117% Analysis Date = 06/16/15 Pct Recovery = 117% Analysis Date = 06/11/15 Pct Recovery = 117% Analysis Date = 06/11/15 Pct Recovery = 117% Analysis Date = 06/06/15 Pct Recovery = 117% Analysis Date = 06/06/15 Pct Recovery = 117% Analysis Date = 06/01/15 Pct Recovery = 117% Analysis Date = 06/01/15 Pct Recovery = 117% Analysis Date = 05/27/15 Pct Recovery = 116% Analysis Date = 05/27/15 Pct Recovery = 116% Analysis Date = 05/23/15 Pct Recovery = 116% Analysis Date = 05/23/15 Pct Recovery = 116% Analysis Date = 05/18/15 Pct Recovery = 116% Analysis Date = 05/18/15 Pct Recovery = 116% Analysis Date = 05/13/15 Pct Recovery = 116% Analysis Date = 05/13/15 Pct Recovery = 116% Analysis Date = 05/08/15 Pct Recovery = 116% Analysis Date = 05/08/15 Pct Recovery = 116% Analysis Date = 05/04/15 Pct Recovery = 116% Analysis Date = 05/04/15 Pct Recovery = 116% Analysis Date = 04/29/15 Pct Recovery = 116% Analysis Date = 04/29/15 Pct Recovery = 116% Analysis Date = 04/24/15 Pct Recovery = 115% Analysis Date = 04/24/15 Pct Recovery = 115% Analysis Date = 04/19/15 Pct Recovery = 115% Analysis Date = 04/19/15 Pct Recovery = 115% Analysis Date = 04/14/15 Pct Recovery = 115% Analysis Date = 04/14/15 Pct Recovery = 115% Analysis Date = 04/10/15 Pct Recovery = 115% Analysis Date = 04/10/15 Pct Recovery = 115% Analysis Date = 04/05/15 Pct Recovery = 115% Analysis Date = 04/05/15 Pct Recovery = 115% Analysis Date = 03/31/15 Pct Recovery = 115% Analysis Date = 03/31/15 Pct Recovery = 115% Analysis Date = 03/26/15 Pct Recovery = 115% Analysis Date = 03/26/15 Pct Recovery = 115% Analysis Date = 03/22/15 Pct Recovery = 115% Analysis Date = 03/22/15 Pct Recovery = 115% Analysis Date = 03/17/15 Pct Recovery = 114% Analysis Date = 03/17/15 Pct Recovery = 114% Analysis Date = 03/12/15 Pct Recovery = 114% Analysis Date = 03/12/15 Pct Recovery = 114% Analysis Date = 03/07/15 Pct Recovery = 114% Analysis Date = 03/07/15 Pct Recovery = 114% Analysis Date = 03/02/15 Pct Recovery = 114% Analysis Date = 03/02/15 Pct Recovery = 114% Analysis Date = 02/26/15 Pct Recovery = 114% Analysis Date = 02/26/15 Pct Recovery = 114% Analysis Date = 02/21/15 Pct Recovery = 114% Analysis Date = 02/21/15 Pct Recovery = 114% Analysis Date = 02/16/15 Pct Recovery = 114% Analysis Date = 02/16/15 Pct Recovery = 114% Analysis Date = 02/11/15 Pct Recovery = 113% Analysis Date = 02/11/15 Pct Recovery = 113% Analysis Date = 02/07/15 Pct Recovery = 113% Analysis Date = 02/07/15 Pct Recovery = 113% Analysis Date = 02/02/15 Pct Recovery = 113% Analysis Date = 02/02/15 Pct Recovery = 113% Analysis Date = 01/28/15 Pct Recovery = 113% Analysis Date = 01/28/15 Pct Recovery = 113% Analysis Date = 01/23/15 Pct Recovery = 113% Analysis Date = 01/23/15 Pct Recovery = 113% Analysis Date = 01/18/15 Pct Recovery = 113% Analysis Date = 01/18/15 Pct Recovery = 113% Analysis Date = 01/14/15 Pct Recovery = 112% Analysis Date = 01/14/15 Pct Recovery = 112% Analysis Date = 01/09/15 Pct Recovery = 112% Analysis Date = 01/09/15 Pct Recovery = 112% Analysis Date = 01/04/15 Pct Recovery = 112% Analysis Date = 01/04/15 Pct Recovery = 112% Analysis Date = 12/30/14 Pct Recovery = 112% Analysis Date = 12/30/14 Pct Recovery = 112% Analysis Date = 12/25/14 Pct Recovery = 112% Analysis Date = 12/25/14 Pct Recovery = 112% Analysis Date = 12/21/14 Pct Recovery = 112% Analysis Date = 12/21/14 Pct Recovery = 112% Analysis Date = 12/16/14 Pct Recovery = 112% Analysis Date = 12/16/14 Pct Recovery = 112% Analysis Date = 12/11/14 Pct Recovery = 111% Analysis Date = 12/11/14 Pct Recovery = 111% Analysis Date = 12/06/14 Pct Recovery = 111% Analysis Date = 12/06/14 Pct Recovery = 111% Analysis Date = 12/02/14 Pct Recovery = 111% Analysis Date = 12/02/14 Pct Recovery = 111% Analysis Date = 11/27/14 Pct Recovery = 111% Analysis Date = 11/27/14 Pct Recovery = 111% Analysis Date = 11/22/14 Pct Recovery = 111% Analysis Date = 11/22/14 Pct Recovery = 111% Analysis Date = 11/17/14 Pct Recovery = 111% Analysis Date = 11/17/14 Pct Recovery = 111% Analysis Date = 11/12/14 Pct Recovery = 111% Analysis Date = 11/12/14 Pct Recovery = 111% Analysis Date = 11/08/14 Pct Recovery = 110% Analysis Date = 11/08/14 Pct Recovery = 110% Analysis Date = 11/03/14 Pct Recovery = 110% Analysis Date = 11/03/14 Pct Recovery = 110% Analysis Date = 10/29/14 Pct Recovery = 110% Analysis Date = 10/29/14 Pct Recovery = 110% Analysis Date = 10/24/14 Pct Recovery = 110% Analysis Date = 10/24/14 Pct Recovery = 110% Analysis Date = 10/20/14 Pct Recovery = 110% Analysis Date = 10/20/14 Pct Recovery = 110% Analysis Date = 10/15/14 Pct Recovery = 109% Analysis Date = 10/15/14 Pct Recovery = 109% Analysis Date = 10/10/14 Pct Recovery = 109% Analysis Date = 10/10/14 Pct Recovery = 109% Analysis Date = 10/05/14 Pct Recovery = 109% Analysis Date = 10/05/14 Pct Recovery = 109% Analysis Date = 09/30/14 Pct Recovery = 109% Analysis Date = 09/30/14 Pct Recovery = 109% Analysis Date = 09/26/14 Pct Recovery = 108% Analysis Date = 09/26/14 Pct Recovery = 108% Analysis Date = 09/21/14 Pct Recovery = 108% Analysis Date = 09/21/14 Pct Recovery = 108% Analysis Date = 09/16/14 Pct Recovery = 108% Analysis Date = 09/16/14 Pct Recovery = 108% Analysis Date = 09/11/14 Pct Recovery = 108% Analysis Date = 09/11/14 Pct Recovery = 108% Analysis Date = 09/07/14 Pct Recovery = 108% Analysis Date = 09/07/14 Pct Recovery = 108% Analysis Date = 09/02/14 Pct Recovery = 107% Analysis Date = 09/02/14 Pct Recovery = 107% Analysis Date = 08/28/14 Pct Recovery = 107% Analysis Date = 08/28/14 Pct Recovery = 107% Analysis Date = 08/23/14 Pct Recovery = 107% Analysis Date = 08/23/14 Pct Recovery = 107% Analysis Date = 08/18/14 Pct Recovery = 107% Analysis Date = 08/18/14 Pct Recovery = 107% Analysis Date = 08/14/14 Pct Recovery = 107% Analysis Date = 08/14/14 Pct Recovery = 107% Analysis Date = 08/09/14 Pct Recovery = 107% Analysis Date = 08/09/14 Pct Recovery = 107% Analysis Date = 08/04/14 Pct Recovery = 106% Analysis Date = 08/04/14 Pct Recovery = 106% Analysis Date = 07/30/14 Pct Recovery = 106% Analysis Date = 07/30/14 Pct Recovery = 106% Analysis Date = 07/26/14 Pct Recovery = 106% Analysis Date = 07/26/14 Pct Recovery = 106% Analysis Date = 07/21/14 Pct Recovery = 106% Analysis Date = 07/21/14 Pct Recovery = 106% Analysis Date = 07/16/14 Pct Recovery = 106% Analysis Date = 07/16/14 Pct Recovery = 106% Analysis Date = 07/11/14 Pct Recovery = 106% Analysis Date = 07/11/14 Pct Recovery = 106% Analysis Date = 07/06/14 Pct Recovery = 105% Analysis Date = 07/06/14 Pct Recovery = 105% Analysis Date = 07/02/14 Pct Recovery = 105% Analysis Date = 07/02/14 Pct Recovery = 105% Analysis Date = 06/27/14 Pct Recovery = 105% Analysis Date = 06/27/14 Pct Recovery = 105% Analysis Date = 06/22/14 Pct Recovery = 105% Analysis Date = 06/22/14 Pct Recovery = 105% Analysis Date = 06/17/14 Pct Recovery = 105% Analysis Date = 06/17/14 Pct Recovery = 105% Analysis Date = 06/13/14 Pct Recovery = 105% Analysis Date = 06/13/14 Pct Recovery = 105% Analysis Date = 06/08/14 Pct Recovery = 105% Analysis Date = 06/08/14 Pct Recovery = 105% Analysis Date = 06/03/14 Pct Recovery = 104% Analysis Date = 06/03/14 Pct Recovery = 104% Analysis Date = 05/29/14 Pct Recovery = 104% Analysis Date = 05/29/14 Pct Recovery = 104% Analysis Date = 05/24/14 Pct Recovery = 104% Analysis Date = 05/24/14 Pct Recovery = 104% Analysis Date = 05/20/14 Pct Recovery = 104% Analysis Date = 05/20/14 Pct Recovery = 104% Analysis Date = 05/15/14 Pct Recovery = 104% Analysis Date = 05/15/14 Pct Recovery = 104% Analysis Date = 05/10/14 Pct Recovery = 104% Analysis Date = 05/10/14 Pct Recovery = 104% Analysis Date = 05/05/14 Pct Recovery = 104% Analysis Date = 05/05/14 Pct Recovery = 104% Analysis Date = 05/01/14 Pct Recovery = 103% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
CHLOROMETHANE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 47 109% 31% 100% 27%
Total 47 109% 31% 100% 27%

Sample Statistics
CHLOROMETHANE

Characteristic N % % Basis
Plotted 47 100% Spiked
Estimated Values 47 100% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 47 .  
False Negatives 0 0% 0 out of 47
Not Spiked 26 .  
False Positives 3 12% 3 out of 26

BQS OBSP Determination:
CIS-1,2-DICHLOROETHYLENE
METHOD: 4440 , TESTIDCODE: 77093GCM66
Open Data Set

Analysis Date = 12/12/16 SpikeMix = Accu 216041125: 40 µl & Crescent 03FF058: 40 µl Pct Recovery = 105% Analysis Date = 08/04/16 SpikeMix = Crescent 03FF058: 40 µl & Supelco LC20141V: 40 µl Pct Recovery = 101% Analysis Date = 11/21/16 SpikeMix = Crescent 03FF058: 25 µl & Supelco LC20141V: 25 µl Pct Recovery = 96% Analysis Date = 06/30/16 SpikeMix = Crescent 03FF058: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 97% Analysis Date = 06/21/16 SpikeMix = Phenova B20160319: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 101% Analysis Date = 05/24/16 SpikeMix = Accu 216041125: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 93% Analysis Date = 08/15/15 SpikeMix = Supelco LC13545: 25 µl & Crescent 04EE008: 25 µl Pct Recovery = 99% Analysis Date = 06/16/15 SpikeMix = ERA 0406-15-03: 25 µl & Supelco LC13545: 25 µl Pct Recovery = 99% Analysis Date = 03/19/15 SpikeMix = Spex Organics C1140417015: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 103% Analysis Date = 12/17/14 SpikeMix = Supelco LC06438: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 95% Analysis Date = 11/14/14 SpikeMix = Crescent 03DD004: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 93% Analysis Date = 06/10/14 SpikeMix = Crescent 03DD004: 20 µl & NSI 032614: 20 µl Pct Recovery = 104% Analysis Date = 04/09/15 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 99% Analysis Date = 08/19/14 SpikeMix = Spex Organics C1140417015: 20 µl & Accu 214031115: 20 µl Pct Recovery = 115% Analysis Date = 07/01/14 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 106% Analysis Date = 05/01/14 SpikeMix = Accu 214031115: 20 µl & NSI 032614: 20 µl Pct Recovery = 101% Analysis Date = 04/26/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 114% Analysis Date = 02/05/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 95% Analysis Date = 11/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 95% Analysis Date = 10/16/15 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 99% Analysis Date = 05/09/15 SpikeMix = Spex Organics EN150428007: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 99% Analysis Date = 09/28/16 SpikeMix = Crescent 03FF058: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 91% Analysis Date = 09/08/16 SpikeMix = Phenova B20160319: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 104% Analysis Date = 08/20/16 SpikeMix = Accu 216041125: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 98% Analysis Date = 04/02/16 SpikeMix = Supelco LC13545: 15 µl & Accu 215041380: 15 µl Pct Recovery = 102% Analysis Date = 12/18/15 SpikeMix = Supelco LC13545: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 95% Analysis Date = 11/06/14 SpikeMix = Spex Organics C1140417015: 10 µl & Crescent 03DD004: 10 µl Pct Recovery = 96% Analysis Date = 10/04/14 SpikeMix = Crescent 03DD004: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 100% Analysis Date = 07/29/14 SpikeMix = Crescent 03DD004: 10 µl & NSI 032614: 10 µl Pct Recovery = 103% Analysis Date = 05/03/14 SpikeMix = Crescent 03DD004: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 105% Analysis Date = 01/13/15 SpikeMix = Accu 214031115: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 106% Analysis Date = 09/09/14 SpikeMix = Accu 214031115: 10 µl & NSI 032614: 10 µl Pct Recovery = 125% Analysis Date = 07/23/14 SpikeMix = Spex Organics C1140417015: 10 µl & Accu 214031115: 10 µl Pct Recovery = 140% Analysis Date = 06/18/14 SpikeMix = Supelco LC06438: 10 µl & Accu 214031115: 10 µl Pct Recovery = 129% Analysis Date = 02/18/16 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 97% Analysis Date = 11/12/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 100% Analysis Date = 09/03/15 SpikeMix = NSI 050515AVOC: 10 µl & Spex Organics EN150428007: 10 µl Pct Recovery = 96% Analysis Date = 05/21/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 104% Analysis Date = 05/13/16 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 100% Analysis Date = 03/17/16 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 99% Analysis Date = 12/10/15 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 102% Analysis Date = 06/27/15 SpikeMix = ERA 0406-15-03: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 102% Analysis Date = 05/09/15 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 102% Analysis Date = 12/11/16 Pct Recovery = 100% Analysis Date = 12/07/16 Pct Recovery = 100% Analysis Date = 12/07/16 Pct Recovery = 100% Analysis Date = 12/02/16 Pct Recovery = 100% Analysis Date = 12/02/16 Pct Recovery = 100% Analysis Date = 11/27/16 Pct Recovery = 100% Analysis Date = 11/27/16 Pct Recovery = 100% Analysis Date = 11/22/16 Pct Recovery = 100% Analysis Date = 11/22/16 Pct Recovery = 100% Analysis Date = 11/18/16 Pct Recovery = 100% Analysis Date = 11/18/16 Pct Recovery = 100% Analysis Date = 11/13/16 Pct Recovery = 100% Analysis Date = 11/13/16 Pct Recovery = 100% Analysis Date = 11/08/16 Pct Recovery = 100% Analysis Date = 11/08/16 Pct Recovery = 100% Analysis Date = 11/03/16 Pct Recovery = 100% Analysis Date = 11/03/16 Pct Recovery = 100% Analysis Date = 10/29/16 Pct Recovery = 100% Analysis Date = 10/29/16 Pct Recovery = 100% Analysis Date = 10/25/16 Pct Recovery = 100% Analysis Date = 10/25/16 Pct Recovery = 100% Analysis Date = 10/20/16 Pct Recovery = 100% Analysis Date = 10/20/16 Pct Recovery = 100% Analysis Date = 10/15/16 Pct Recovery = 100% Analysis Date = 10/15/16 Pct Recovery = 100% Analysis Date = 10/10/16 Pct Recovery = 100% Analysis Date = 10/10/16 Pct Recovery = 100% Analysis Date = 10/06/16 Pct Recovery = 100% Analysis Date = 10/06/16 Pct Recovery = 100% Analysis Date = 10/01/16 Pct Recovery = 100% Analysis Date = 10/01/16 Pct Recovery = 100% Analysis Date = 09/26/16 Pct Recovery = 100% Analysis Date = 09/26/16 Pct Recovery = 100% Analysis Date = 09/21/16 Pct Recovery = 100% Analysis Date = 09/21/16 Pct Recovery = 100% Analysis Date = 09/16/16 Pct Recovery = 100% Analysis Date = 09/16/16 Pct Recovery = 100% Analysis Date = 09/12/16 Pct Recovery = 100% Analysis Date = 09/12/16 Pct Recovery = 100% Analysis Date = 09/07/16 Pct Recovery = 100% Analysis Date = 09/07/16 Pct Recovery = 100% Analysis Date = 09/02/16 Pct Recovery = 100% Analysis Date = 09/02/16 Pct Recovery = 100% Analysis Date = 08/28/16 Pct Recovery = 100% Analysis Date = 08/28/16 Pct Recovery = 100% Analysis Date = 08/24/16 Pct Recovery = 100% Analysis Date = 08/24/16 Pct Recovery = 100% Analysis Date = 08/19/16 Pct Recovery = 100% Analysis Date = 08/19/16 Pct Recovery = 100% Analysis Date = 08/14/16 Pct Recovery = 100% Analysis Date = 08/14/16 Pct Recovery = 100% Analysis Date = 08/09/16 Pct Recovery = 100% Analysis Date = 08/09/16 Pct Recovery = 100% Analysis Date = 08/04/16 Pct Recovery = 100% Analysis Date = 08/04/16 Pct Recovery = 100% Analysis Date = 07/31/16 Pct Recovery = 100% Analysis Date = 07/31/16 Pct Recovery = 100% Analysis Date = 07/26/16 Pct Recovery = 100% Analysis Date = 07/26/16 Pct Recovery = 100% Analysis Date = 07/21/16 Pct Recovery = 99% Analysis Date = 07/21/16 Pct Recovery = 99% Analysis Date = 07/16/16 Pct Recovery = 99% Analysis Date = 07/16/16 Pct Recovery = 99% Analysis Date = 07/12/16 Pct Recovery = 99% Analysis Date = 07/12/16 Pct Recovery = 99% Analysis Date = 07/07/16 Pct Recovery = 99% Analysis Date = 07/07/16 Pct Recovery = 99% Analysis Date = 07/02/16 Pct Recovery = 99% Analysis Date = 07/02/16 Pct Recovery = 99% Analysis Date = 06/27/16 Pct Recovery = 99% Analysis Date = 06/27/16 Pct Recovery = 99% Analysis Date = 06/22/16 Pct Recovery = 99% Analysis Date = 06/22/16 Pct Recovery = 99% Analysis Date = 06/18/16 Pct Recovery = 99% Analysis Date = 06/18/16 Pct Recovery = 99% Analysis Date = 06/13/16 Pct Recovery = 99% Analysis Date = 06/13/16 Pct Recovery = 99% Analysis Date = 06/08/16 Pct Recovery = 99% Analysis Date = 06/08/16 Pct Recovery = 99% Analysis Date = 06/03/16 Pct Recovery = 99% Analysis Date = 06/03/16 Pct Recovery = 99% Analysis Date = 05/30/16 Pct Recovery = 99% Analysis Date = 05/30/16 Pct Recovery = 99% Analysis Date = 05/25/16 Pct Recovery = 99% Analysis Date = 05/25/16 Pct Recovery = 99% Analysis Date = 05/20/16 Pct Recovery = 99% Analysis Date = 05/20/16 Pct Recovery = 99% Analysis Date = 05/15/16 Pct Recovery = 99% Analysis Date = 05/15/16 Pct Recovery = 99% Analysis Date = 05/10/16 Pct Recovery = 99% Analysis Date = 05/10/16 Pct Recovery = 99% Analysis Date = 05/06/16 Pct Recovery = 99% Analysis Date = 05/06/16 Pct Recovery = 99% Analysis Date = 05/01/16 Pct Recovery = 99% Analysis Date = 05/01/16 Pct Recovery = 99% Analysis Date = 04/26/16 Pct Recovery = 99% Analysis Date = 04/26/16 Pct Recovery = 99% Analysis Date = 04/21/16 Pct Recovery = 99% Analysis Date = 04/21/16 Pct Recovery = 99% Analysis Date = 04/16/16 Pct Recovery = 99% Analysis Date = 04/16/16 Pct Recovery = 99% Analysis Date = 04/12/16 Pct Recovery = 99% Analysis Date = 04/12/16 Pct Recovery = 99% Analysis Date = 04/07/16 Pct Recovery = 99% Analysis Date = 04/07/16 Pct Recovery = 99% Analysis Date = 04/02/16 Pct Recovery = 99% Analysis Date = 04/02/16 Pct Recovery = 99% Analysis Date = 03/28/16 Pct Recovery = 99% Analysis Date = 03/28/16 Pct Recovery = 99% Analysis Date = 03/24/16 Pct Recovery = 99% Analysis Date = 03/24/16 Pct Recovery = 99% Analysis Date = 03/19/16 Pct Recovery = 99% Analysis Date = 03/19/16 Pct Recovery = 99% Analysis Date = 03/14/16 Pct Recovery = 99% Analysis Date = 03/14/16 Pct Recovery = 99% Analysis Date = 03/09/16 Pct Recovery = 99% Analysis Date = 03/09/16 Pct Recovery = 99% Analysis Date = 03/04/16 Pct Recovery = 99% Analysis Date = 03/04/16 Pct Recovery = 99% Analysis Date = 02/29/16 Pct Recovery = 99% Analysis Date = 02/29/16 Pct Recovery = 99% Analysis Date = 02/24/16 Pct Recovery = 99% Analysis Date = 02/24/16 Pct Recovery = 99% Analysis Date = 02/19/16 Pct Recovery = 99% Analysis Date = 02/19/16 Pct Recovery = 99% Analysis Date = 02/14/16 Pct Recovery = 99% Analysis Date = 02/14/16 Pct Recovery = 99% Analysis Date = 02/10/16 Pct Recovery = 99% Analysis Date = 02/10/16 Pct Recovery = 99% Analysis Date = 02/05/16 Pct Recovery = 99% Analysis Date = 02/05/16 Pct Recovery = 99% Analysis Date = 01/31/16 Pct Recovery = 99% Analysis Date = 01/31/16 Pct Recovery = 99% Analysis Date = 01/26/16 Pct Recovery = 99% Analysis Date = 01/26/16 Pct Recovery = 99% Analysis Date = 01/21/16 Pct Recovery = 99% Analysis Date = 01/21/16 Pct Recovery = 99% Analysis Date = 01/17/16 Pct Recovery = 99% Analysis Date = 01/17/16 Pct Recovery = 99% Analysis Date = 01/12/16 Pct Recovery = 99% Analysis Date = 01/12/16 Pct Recovery = 99% Analysis Date = 01/07/16 Pct Recovery = 99% Analysis Date = 01/07/16 Pct Recovery = 99% Analysis Date = 01/02/16 Pct Recovery = 99% Analysis Date = 01/02/16 Pct Recovery = 99% Analysis Date = 12/29/15 Pct Recovery = 99% Analysis Date = 12/29/15 Pct Recovery = 99% Analysis Date = 12/24/15 Pct Recovery = 99% Analysis Date = 12/24/15 Pct Recovery = 99% Analysis Date = 12/19/15 Pct Recovery = 99% Analysis Date = 12/19/15 Pct Recovery = 99% Analysis Date = 12/14/15 Pct Recovery = 99% Analysis Date = 12/14/15 Pct Recovery = 99% Analysis Date = 12/09/15 Pct Recovery = 99% Analysis Date = 12/09/15 Pct Recovery = 99% Analysis Date = 12/05/15 Pct Recovery = 99% Analysis Date = 12/05/15 Pct Recovery = 99% Analysis Date = 11/30/15 Pct Recovery = 99% Analysis Date = 11/30/15 Pct Recovery = 99% Analysis Date = 11/25/15 Pct Recovery = 99% Analysis Date = 11/25/15 Pct Recovery = 99% Analysis Date = 11/20/15 Pct Recovery = 99% Analysis Date = 11/20/15 Pct Recovery = 99% Analysis Date = 11/16/15 Pct Recovery = 99% Analysis Date = 11/16/15 Pct Recovery = 99% Analysis Date = 11/11/15 Pct Recovery = 99% Analysis Date = 11/11/15 Pct Recovery = 99% Analysis Date = 11/06/15 Pct Recovery = 99% Analysis Date = 11/06/15 Pct Recovery = 99% Analysis Date = 11/01/15 Pct Recovery = 99% Analysis Date = 11/01/15 Pct Recovery = 99% Analysis Date = 10/27/15 Pct Recovery = 99% Analysis Date = 10/27/15 Pct Recovery = 99% Analysis Date = 10/23/15 Pct Recovery = 99% Analysis Date = 10/23/15 Pct Recovery = 99% Analysis Date = 10/18/15 Pct Recovery = 99% Analysis Date = 10/18/15 Pct Recovery = 99% Analysis Date = 10/13/15 Pct Recovery = 99% Analysis Date = 10/13/15 Pct Recovery = 99% Analysis Date = 10/08/15 Pct Recovery = 99% Analysis Date = 10/08/15 Pct Recovery = 99% Analysis Date = 10/04/15 Pct Recovery = 99% Analysis Date = 10/04/15 Pct Recovery = 99% Analysis Date = 09/29/15 Pct Recovery = 99% Analysis Date = 09/29/15 Pct Recovery = 99% Analysis Date = 09/24/15 Pct Recovery = 99% Analysis Date = 09/24/15 Pct Recovery = 99% Analysis Date = 09/19/15 Pct Recovery = 99% Analysis Date = 09/19/15 Pct Recovery = 99% Analysis Date = 09/14/15 Pct Recovery = 99% Analysis Date = 09/14/15 Pct Recovery = 99% Analysis Date = 09/10/15 Pct Recovery = 99% Analysis Date = 09/10/15 Pct Recovery = 99% Analysis Date = 09/05/15 Pct Recovery = 99% Analysis Date = 09/05/15 Pct Recovery = 99% Analysis Date = 08/31/15 Pct Recovery = 99% Analysis Date = 08/31/15 Pct Recovery = 99% Analysis Date = 08/26/15 Pct Recovery = 99% Analysis Date = 08/26/15 Pct Recovery = 99% Analysis Date = 08/21/15 Pct Recovery = 99% Analysis Date = 08/21/15 Pct Recovery = 99% Analysis Date = 08/17/15 Pct Recovery = 99% Analysis Date = 08/17/15 Pct Recovery = 99% Analysis Date = 08/12/15 Pct Recovery = 99% Analysis Date = 08/12/15 Pct Recovery = 99% Analysis Date = 08/07/15 Pct Recovery = 100% Analysis Date = 08/07/15 Pct Recovery = 100% Analysis Date = 08/02/15 Pct Recovery = 100% Analysis Date = 08/02/15 Pct Recovery = 100% Analysis Date = 07/29/15 Pct Recovery = 100% Analysis Date = 07/29/15 Pct Recovery = 100% Analysis Date = 07/24/15 Pct Recovery = 100% Analysis Date = 07/24/15 Pct Recovery = 100% Analysis Date = 07/19/15 Pct Recovery = 100% Analysis Date = 07/19/15 Pct Recovery = 100% Analysis Date = 07/14/15 Pct Recovery = 100% Analysis Date = 07/14/15 Pct Recovery = 100% Analysis Date = 07/09/15 Pct Recovery = 100% Analysis Date = 07/09/15 Pct Recovery = 100% Analysis Date = 07/05/15 Pct Recovery = 100% Analysis Date = 07/05/15 Pct Recovery = 100% Analysis Date = 06/30/15 Pct Recovery = 100% Analysis Date = 06/30/15 Pct Recovery = 100% Analysis Date = 06/25/15 Pct Recovery = 100% Analysis Date = 06/25/15 Pct Recovery = 100% Analysis Date = 06/20/15 Pct Recovery = 100% Analysis Date = 06/20/15 Pct Recovery = 100% Analysis Date = 06/16/15 Pct Recovery = 100% Analysis Date = 06/16/15 Pct Recovery = 100% Analysis Date = 06/11/15 Pct Recovery = 100% Analysis Date = 06/11/15 Pct Recovery = 100% Analysis Date = 06/06/15 Pct Recovery = 100% Analysis Date = 06/06/15 Pct Recovery = 100% Analysis Date = 06/01/15 Pct Recovery = 100% Analysis Date = 06/01/15 Pct Recovery = 100% Analysis Date = 05/27/15 Pct Recovery = 100% Analysis Date = 05/27/15 Pct Recovery = 100% Analysis Date = 05/23/15 Pct Recovery = 100% Analysis Date = 05/23/15 Pct Recovery = 100% Analysis Date = 05/18/15 Pct Recovery = 100% Analysis Date = 05/18/15 Pct Recovery = 100% Analysis Date = 05/13/15 Pct Recovery = 100% Analysis Date = 05/13/15 Pct Recovery = 100% Analysis Date = 05/08/15 Pct Recovery = 100% Analysis Date = 05/08/15 Pct Recovery = 100% Analysis Date = 05/04/15 Pct Recovery = 100% Analysis Date = 05/04/15 Pct Recovery = 100% Analysis Date = 04/29/15 Pct Recovery = 100% Analysis Date = 04/29/15 Pct Recovery = 100% Analysis Date = 04/24/15 Pct Recovery = 100% Analysis Date = 04/24/15 Pct Recovery = 100% Analysis Date = 04/19/15 Pct Recovery = 101% Analysis Date = 04/19/15 Pct Recovery = 101% Analysis Date = 04/14/15 Pct Recovery = 101% Analysis Date = 04/14/15 Pct Recovery = 101% Analysis Date = 04/10/15 Pct Recovery = 101% Analysis Date = 04/10/15 Pct Recovery = 101% Analysis Date = 04/05/15 Pct Recovery = 101% Analysis Date = 04/05/15 Pct Recovery = 101% Analysis Date = 03/31/15 Pct Recovery = 101% Analysis Date = 03/31/15 Pct Recovery = 101% Analysis Date = 03/26/15 Pct Recovery = 101% Analysis Date = 03/26/15 Pct Recovery = 101% Analysis Date = 03/22/15 Pct Recovery = 102% Analysis Date = 03/22/15 Pct Recovery = 102% Analysis Date = 03/17/15 Pct Recovery = 102% Analysis Date = 03/17/15 Pct Recovery = 102% Analysis Date = 03/12/15 Pct Recovery = 102% Analysis Date = 03/12/15 Pct Recovery = 102% Analysis Date = 03/07/15 Pct Recovery = 102% Analysis Date = 03/07/15 Pct Recovery = 102% Analysis Date = 03/02/15 Pct Recovery = 102% Analysis Date = 03/02/15 Pct Recovery = 102% Analysis Date = 02/26/15 Pct Recovery = 102% Analysis Date = 02/26/15 Pct Recovery = 102% Analysis Date = 02/21/15 Pct Recovery = 103% Analysis Date = 02/21/15 Pct Recovery = 103% Analysis Date = 02/16/15 Pct Recovery = 103% Analysis Date = 02/16/15 Pct Recovery = 103% Analysis Date = 02/11/15 Pct Recovery = 103% Analysis Date = 02/11/15 Pct Recovery = 103% Analysis Date = 02/07/15 Pct Recovery = 103% Analysis Date = 02/07/15 Pct Recovery = 103% Analysis Date = 02/02/15 Pct Recovery = 103% Analysis Date = 02/02/15 Pct Recovery = 103% Analysis Date = 01/28/15 Pct Recovery = 103% Analysis Date = 01/28/15 Pct Recovery = 103% Analysis Date = 01/23/15 Pct Recovery = 103% Analysis Date = 01/23/15 Pct Recovery = 103% Analysis Date = 01/18/15 Pct Recovery = 104% Analysis Date = 01/18/15 Pct Recovery = 104% Analysis Date = 01/14/15 Pct Recovery = 104% Analysis Date = 01/14/15 Pct Recovery = 104% Analysis Date = 01/09/15 Pct Recovery = 104% Analysis Date = 01/09/15 Pct Recovery = 104% Analysis Date = 01/04/15 Pct Recovery = 104% Analysis Date = 01/04/15 Pct Recovery = 104% Analysis Date = 12/30/14 Pct Recovery = 104% Analysis Date = 12/30/14 Pct Recovery = 104% Analysis Date = 12/25/14 Pct Recovery = 105% Analysis Date = 12/25/14 Pct Recovery = 105% Analysis Date = 12/21/14 Pct Recovery = 105% Analysis Date = 12/21/14 Pct Recovery = 105% Analysis Date = 12/16/14 Pct Recovery = 105% Analysis Date = 12/16/14 Pct Recovery = 105% Analysis Date = 12/11/14 Pct Recovery = 105% Analysis Date = 12/11/14 Pct Recovery = 105% Analysis Date = 12/06/14 Pct Recovery = 105% Analysis Date = 12/06/14 Pct Recovery = 105% Analysis Date = 12/02/14 Pct Recovery = 105% Analysis Date = 12/02/14 Pct Recovery = 105% Analysis Date = 11/27/14 Pct Recovery = 106% Analysis Date = 11/27/14 Pct Recovery = 106% Analysis Date = 11/22/14 Pct Recovery = 106% Analysis Date = 11/22/14 Pct Recovery = 106% Analysis Date = 11/17/14 Pct Recovery = 106% Analysis Date = 11/17/14 Pct Recovery = 106% Analysis Date = 11/12/14 Pct Recovery = 106% Analysis Date = 11/12/14 Pct Recovery = 106% Analysis Date = 11/08/14 Pct Recovery = 106% Analysis Date = 11/08/14 Pct Recovery = 106% Analysis Date = 11/03/14 Pct Recovery = 107% Analysis Date = 11/03/14 Pct Recovery = 107% Analysis Date = 10/29/14 Pct Recovery = 107% Analysis Date = 10/29/14 Pct Recovery = 107% Analysis Date = 10/24/14 Pct Recovery = 107% Analysis Date = 10/24/14 Pct Recovery = 107% Analysis Date = 10/20/14 Pct Recovery = 107% Analysis Date = 10/20/14 Pct Recovery = 107% Analysis Date = 10/15/14 Pct Recovery = 107% Analysis Date = 10/15/14 Pct Recovery = 107% Analysis Date = 10/10/14 Pct Recovery = 107% Analysis Date = 10/10/14 Pct Recovery = 107% Analysis Date = 10/05/14 Pct Recovery = 107% Analysis Date = 10/05/14 Pct Recovery = 107% Analysis Date = 09/30/14 Pct Recovery = 108% Analysis Date = 09/30/14 Pct Recovery = 108% Analysis Date = 09/26/14 Pct Recovery = 108% Analysis Date = 09/26/14 Pct Recovery = 108% Analysis Date = 09/21/14 Pct Recovery = 108% Analysis Date = 09/21/14 Pct Recovery = 108% Analysis Date = 09/16/14 Pct Recovery = 108% Analysis Date = 09/16/14 Pct Recovery = 108% Analysis Date = 09/11/14 Pct Recovery = 108% Analysis Date = 09/11/14 Pct Recovery = 108% Analysis Date = 09/07/14 Pct Recovery = 108% Analysis Date = 09/07/14 Pct Recovery = 108% Analysis Date = 09/02/14 Pct Recovery = 109% Analysis Date = 09/02/14 Pct Recovery = 109% Analysis Date = 08/28/14 Pct Recovery = 109% Analysis Date = 08/28/14 Pct Recovery = 109% Analysis Date = 08/23/14 Pct Recovery = 109% Analysis Date = 08/23/14 Pct Recovery = 109% Analysis Date = 08/18/14 Pct Recovery = 109% Analysis Date = 08/18/14 Pct Recovery = 109% Analysis Date = 08/14/14 Pct Recovery = 109% Analysis Date = 08/14/14 Pct Recovery = 109% Analysis Date = 08/09/14 Pct Recovery = 109% Analysis Date = 08/09/14 Pct Recovery = 109% Analysis Date = 08/04/14 Pct Recovery = 110% Analysis Date = 08/04/14 Pct Recovery = 110% Analysis Date = 07/30/14 Pct Recovery = 110% Analysis Date = 07/30/14 Pct Recovery = 110% Analysis Date = 07/26/14 Pct Recovery = 110% Analysis Date = 07/26/14 Pct Recovery = 110% Analysis Date = 07/21/14 Pct Recovery = 110% Analysis Date = 07/21/14 Pct Recovery = 110% Analysis Date = 07/16/14 Pct Recovery = 110% Analysis Date = 07/16/14 Pct Recovery = 110% Analysis Date = 07/11/14 Pct Recovery = 110% Analysis Date = 07/11/14 Pct Recovery = 110% Analysis Date = 07/06/14 Pct Recovery = 111% Analysis Date = 07/06/14 Pct Recovery = 111% Analysis Date = 07/02/14 Pct Recovery = 111% Analysis Date = 07/02/14 Pct Recovery = 111% Analysis Date = 06/27/14 Pct Recovery = 111% Analysis Date = 06/27/14 Pct Recovery = 111% Analysis Date = 06/22/14 Pct Recovery = 111% Analysis Date = 06/22/14 Pct Recovery = 111% Analysis Date = 06/17/14 Pct Recovery = 111% Analysis Date = 06/17/14 Pct Recovery = 111% Analysis Date = 06/13/14 Pct Recovery = 112% Analysis Date = 06/13/14 Pct Recovery = 112% Analysis Date = 06/08/14 Pct Recovery = 112% Analysis Date = 06/08/14 Pct Recovery = 112% Analysis Date = 06/03/14 Pct Recovery = 112% Analysis Date = 06/03/14 Pct Recovery = 112% Analysis Date = 05/29/14 Pct Recovery = 112% Analysis Date = 05/29/14 Pct Recovery = 112% Analysis Date = 05/24/14 Pct Recovery = 112% Analysis Date = 05/24/14 Pct Recovery = 112% Analysis Date = 05/20/14 Pct Recovery = 112% Analysis Date = 05/20/14 Pct Recovery = 112% Analysis Date = 05/15/14 Pct Recovery = 113% Analysis Date = 05/15/14 Pct Recovery = 113% Analysis Date = 05/10/14 Pct Recovery = 113% Analysis Date = 05/10/14 Pct Recovery = 113% Analysis Date = 05/05/14 Pct Recovery = 113% Analysis Date = 05/05/14 Pct Recovery = 113% Analysis Date = 05/01/14 Pct Recovery = 113% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
CIS-1,2-DICHLOROETHYLENE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 43 102% 9% 100% 5%
Total 43 102% 9% 100% 5%

Sample Statistics
CIS-1,2-DICHLOROETHYLENE

Characteristic N % % Basis
Plotted 43 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 43 .  
False Negatives 0 0% 0 out of 43
Not Spiked 23 .  
False Positives 0 0% 0 out of 23

BQS OBSP Determination:
CIS-1,3-DICHLOROPROPENE
METHOD: 4440 , TESTIDCODE: 34704GCM66
Open Data Set

Analysis Date = 12/16/16 SpikeMix = NSI 041816AVOC: 40 µl & ChemService 5082900: 40 µl Pct Recovery = 92% Analysis Date = 07/14/16 SpikeMix = Accu 216041125: 40 µl & NSI 041816AVOC: 40 µl Pct Recovery = 98% Analysis Date = 12/12/16 SpikeMix = Accu 216041125: 40 µl & Crescent 03FF058: 40 µl Pct Recovery = 81% Analysis Date = 08/04/16 SpikeMix = Crescent 03FF058: 40 µl & Supelco LC20141V: 40 µl Pct Recovery = 73% Analysis Date = 08/26/16 SpikeMix = NSI 041816AVOC: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 86% Analysis Date = 11/21/16 SpikeMix = Crescent 03FF058: 25 µl & Supelco LC20141V: 25 µl Pct Recovery = 71% Analysis Date = 06/30/16 SpikeMix = Crescent 03FF058: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 76% Analysis Date = 06/21/16 SpikeMix = Phenova B20160319: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 80% Analysis Date = 05/24/16 SpikeMix = Accu 216041125: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 74% Analysis Date = 03/06/15 SpikeMix = ERA 0227-14-06.1A: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 85% Analysis Date = 12/17/14 SpikeMix = Supelco LC06438: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 91% Analysis Date = 09/21/14 SpikeMix = Supelco LC06438: 20 µl Pct Recovery = 98% Analysis Date = 06/10/14 SpikeMix = NSI 032614: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 92% Analysis Date = 03/19/15 SpikeMix = Spex Organics C1140417015: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 48% Analysis Date = 11/22/14 SpikeMix = NSI 032614: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 49% Analysis Date = 08/19/14 SpikeMix = Spex Organics C1140417015: 20 µl & Accu 214031115: 20 µl Pct Recovery = 54% Analysis Date = 08/16/14 SpikeMix = ERA 0227-14-06.1A: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 47% Analysis Date = 08/15/15 SpikeMix = Supelco LC13545: 25 µl & Crescent 04EE008: 25 µl Pct Recovery = 84% Analysis Date = 06/16/15 SpikeMix = ERA 0406-15-03: 25 µl & Supelco LC13545: 25 µl Pct Recovery = 72% Analysis Date = 10/13/16 SpikeMix = Accu 216041125: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 127% Analysis Date = 10/13/16 SpikeMix = NSI 041816AVOC: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 100% Analysis Date = 07/29/16 SpikeMix = Phenova B20160319: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 110% Analysis Date = 06/15/16 SpikeMix = NSI 041816AVOC: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 94% Analysis Date = 09/28/16 SpikeMix = Crescent 03FF058: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 73% Analysis Date = 09/08/16 SpikeMix = Phenova B20160319: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 88% Analysis Date = 08/20/16 SpikeMix = Accu 216041125: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 89% Analysis Date = 04/26/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 98% Analysis Date = 02/05/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 82% Analysis Date = 11/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 104% Analysis Date = 10/16/15 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 102% Analysis Date = 05/09/15 SpikeMix = Spex Organics EN150428007: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 108% Analysis Date = 04/02/16 SpikeMix = Supelco LC13545: 15 µl & Accu 215041380: 15 µl Pct Recovery = 102% Analysis Date = 12/18/15 SpikeMix = Supelco LC13545: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 100% Analysis Date = 10/21/14 SpikeMix = ERA 0227-14-06.1A: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 95% Analysis Date = 06/18/14 SpikeMix = Supelco LC06438: 10 µl & Accu 214031115: 10 µl Pct Recovery = 116% Analysis Date = 05/30/14 SpikeMix = NSI 032614: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 104% Analysis Date = 05/03/14 SpikeMix = Crescent 03DD004: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 115% Analysis Date = 11/06/14 SpikeMix = Spex Organics C1140417015: 10 µl & Crescent 03DD004: 10 µl Pct Recovery = 50% Analysis Date = 09/09/14 SpikeMix = NSI 032614: 10 µl & Spex Organics C1140417015: 10 µl Pct Recovery = 51% Analysis Date = 07/23/14 SpikeMix = Spex Organics C1140417015: 10 µl & Accu 214031115: 10 µl Pct Recovery = 45% Analysis Date = 07/11/14 SpikeMix = Spex Organics C1140417015: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 45% Analysis Date = 02/18/16 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 109% Analysis Date = 11/12/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 108% Analysis Date = 09/03/15 SpikeMix = NSI 050515AVOC: 10 µl & Spex Organics EN150428007: 10 µl Pct Recovery = 102% Analysis Date = 05/21/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 108% Analysis Date = 05/13/16 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 107% Analysis Date = 03/17/16 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 114% Analysis Date = 12/10/15 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 85% Analysis Date = 06/27/15 SpikeMix = ERA 0406-15-03: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 85% Analysis Date = 05/09/15 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 105% Analysis Date = 12/16/16 Pct Recovery = 86% Analysis Date = 12/11/16 Pct Recovery = 87% Analysis Date = 12/11/16 Pct Recovery = 87% Analysis Date = 12/06/16 Pct Recovery = 87% Analysis Date = 12/06/16 Pct Recovery = 87% Analysis Date = 12/01/16 Pct Recovery = 87% Analysis Date = 12/01/16 Pct Recovery = 87% Analysis Date = 11/26/16 Pct Recovery = 87% Analysis Date = 11/26/16 Pct Recovery = 87% Analysis Date = 11/22/16 Pct Recovery = 87% Analysis Date = 11/22/16 Pct Recovery = 87% Analysis Date = 11/17/16 Pct Recovery = 87% Analysis Date = 11/17/16 Pct Recovery = 87% Analysis Date = 11/12/16 Pct Recovery = 88% Analysis Date = 11/12/16 Pct Recovery = 88% Analysis Date = 11/07/16 Pct Recovery = 88% Analysis Date = 11/07/16 Pct Recovery = 88% Analysis Date = 11/02/16 Pct Recovery = 88% Analysis Date = 11/02/16 Pct Recovery = 88% Analysis Date = 10/29/16 Pct Recovery = 88% Analysis Date = 10/29/16 Pct Recovery = 88% Analysis Date = 10/24/16 Pct Recovery = 88% Analysis Date = 10/24/16 Pct Recovery = 88% Analysis Date = 10/19/16 Pct Recovery = 88% Analysis Date = 10/19/16 Pct Recovery = 88% Analysis Date = 10/14/16 Pct Recovery = 89% Analysis Date = 10/14/16 Pct Recovery = 89% Analysis Date = 10/09/16 Pct Recovery = 89% Analysis Date = 10/09/16 Pct Recovery = 89% Analysis Date = 10/05/16 Pct Recovery = 89% Analysis Date = 10/05/16 Pct Recovery = 89% Analysis Date = 09/30/16 Pct Recovery = 89% Analysis Date = 09/30/16 Pct Recovery = 89% Analysis Date = 09/25/16 Pct Recovery = 89% Analysis Date = 09/25/16 Pct Recovery = 89% Analysis Date = 09/20/16 Pct Recovery = 89% Analysis Date = 09/20/16 Pct Recovery = 89% Analysis Date = 09/15/16 Pct Recovery = 90% Analysis Date = 09/15/16 Pct Recovery = 90% Analysis Date = 09/11/16 Pct Recovery = 90% Analysis Date = 09/11/16 Pct Recovery = 90% Analysis Date = 09/06/16 Pct Recovery = 90% Analysis Date = 09/06/16 Pct Recovery = 90% Analysis Date = 09/01/16 Pct Recovery = 90% Analysis Date = 09/01/16 Pct Recovery = 90% Analysis Date = 08/27/16 Pct Recovery = 90% Analysis Date = 08/27/16 Pct Recovery = 90% Analysis Date = 08/23/16 Pct Recovery = 90% Analysis Date = 08/23/16 Pct Recovery = 90% Analysis Date = 08/18/16 Pct Recovery = 91% Analysis Date = 08/18/16 Pct Recovery = 91% Analysis Date = 08/13/16 Pct Recovery = 91% Analysis Date = 08/13/16 Pct Recovery = 91% Analysis Date = 08/08/16 Pct Recovery = 91% Analysis Date = 08/08/16 Pct Recovery = 91% Analysis Date = 08/03/16 Pct Recovery = 91% Analysis Date = 08/03/16 Pct Recovery = 91% Analysis Date = 07/30/16 Pct Recovery = 91% Analysis Date = 07/30/16 Pct Recovery = 91% Analysis Date = 07/25/16 Pct Recovery = 91% Analysis Date = 07/25/16 Pct Recovery = 91% Analysis Date = 07/20/16 Pct Recovery = 92% Analysis Date = 07/20/16 Pct Recovery = 92% Analysis Date = 07/15/16 Pct Recovery = 92% Analysis Date = 07/15/16 Pct Recovery = 92% Analysis Date = 07/10/16 Pct Recovery = 92% Analysis Date = 07/10/16 Pct Recovery = 92% Analysis Date = 07/06/16 Pct Recovery = 92% Analysis Date = 07/06/16 Pct Recovery = 92% Analysis Date = 07/01/16 Pct Recovery = 92% Analysis Date = 07/01/16 Pct Recovery = 92% Analysis Date = 06/26/16 Pct Recovery = 92% Analysis Date = 06/26/16 Pct Recovery = 92% Analysis Date = 06/21/16 Pct Recovery = 93% Analysis Date = 06/21/16 Pct Recovery = 93% Analysis Date = 06/16/16 Pct Recovery = 93% Analysis Date = 06/16/16 Pct Recovery = 93% Analysis Date = 06/12/16 Pct Recovery = 93% Analysis Date = 06/12/16 Pct Recovery = 93% Analysis Date = 06/07/16 Pct Recovery = 93% Analysis Date = 06/07/16 Pct Recovery = 93% Analysis Date = 06/02/16 Pct Recovery = 93% Analysis Date = 06/02/16 Pct Recovery = 93% Analysis Date = 05/28/16 Pct Recovery = 93% Analysis Date = 05/28/16 Pct Recovery = 93% Analysis Date = 05/24/16 Pct Recovery = 94% Analysis Date = 05/24/16 Pct Recovery = 94% Analysis Date = 05/19/16 Pct Recovery = 94% Analysis Date = 05/19/16 Pct Recovery = 94% Analysis Date = 05/14/16 Pct Recovery = 94% Analysis Date = 05/14/16 Pct Recovery = 94% Analysis Date = 05/09/16 Pct Recovery = 94% Analysis Date = 05/09/16 Pct Recovery = 94% Analysis Date = 05/04/16 Pct Recovery = 94% Analysis Date = 05/04/16 Pct Recovery = 94% Analysis Date = 04/30/16 Pct Recovery = 94% Analysis Date = 04/30/16 Pct Recovery = 94% Analysis Date = 04/25/16 Pct Recovery = 95% Analysis Date = 04/25/16 Pct Recovery = 95% Analysis Date = 04/20/16 Pct Recovery = 95% Analysis Date = 04/20/16 Pct Recovery = 95% Analysis Date = 04/15/16 Pct Recovery = 95% Analysis Date = 04/15/16 Pct Recovery = 95% Analysis Date = 04/10/16 Pct Recovery = 95% Analysis Date = 04/10/16 Pct Recovery = 95% Analysis Date = 04/06/16 Pct Recovery = 95% Analysis Date = 04/06/16 Pct Recovery = 95% Analysis Date = 04/01/16 Pct Recovery = 95% Analysis Date = 04/01/16 Pct Recovery = 95% Analysis Date = 03/27/16 Pct Recovery = 95% Analysis Date = 03/27/16 Pct Recovery = 95% Analysis Date = 03/22/16 Pct Recovery = 96% Analysis Date = 03/22/16 Pct Recovery = 96% Analysis Date = 03/17/16 Pct Recovery = 96% Analysis Date = 03/17/16 Pct Recovery = 96% Analysis Date = 03/13/16 Pct Recovery = 96% Analysis Date = 03/13/16 Pct Recovery = 96% Analysis Date = 03/08/16 Pct Recovery = 96% Analysis Date = 03/08/16 Pct Recovery = 96% Analysis Date = 03/03/16 Pct Recovery = 96% Analysis Date = 03/03/16 Pct Recovery = 96% Analysis Date = 02/27/16 Pct Recovery = 96% Analysis Date = 02/27/16 Pct Recovery = 96% Analysis Date = 02/23/16 Pct Recovery = 96% Analysis Date = 02/23/16 Pct Recovery = 96% Analysis Date = 02/18/16 Pct Recovery = 96% Analysis Date = 02/18/16 Pct Recovery = 96% Analysis Date = 02/13/16 Pct Recovery = 96% Analysis Date = 02/13/16 Pct Recovery = 96% Analysis Date = 02/08/16 Pct Recovery = 97% Analysis Date = 02/08/16 Pct Recovery = 97% Analysis Date = 02/03/16 Pct Recovery = 97% Analysis Date = 02/03/16 Pct Recovery = 97% Analysis Date = 01/30/16 Pct Recovery = 97% Analysis Date = 01/30/16 Pct Recovery = 97% Analysis Date = 01/25/16 Pct Recovery = 97% Analysis Date = 01/25/16 Pct Recovery = 97% Analysis Date = 01/20/16 Pct Recovery = 97% Analysis Date = 01/20/16 Pct Recovery = 97% Analysis Date = 01/15/16 Pct Recovery = 96% Analysis Date = 01/15/16 Pct Recovery = 96% Analysis Date = 01/10/16 Pct Recovery = 96% Analysis Date = 01/10/16 Pct Recovery = 96% Analysis Date = 01/06/16 Pct Recovery = 96% Analysis Date = 01/06/16 Pct Recovery = 96% Analysis Date = 01/01/16 Pct Recovery = 96% Analysis Date = 01/01/16 Pct Recovery = 96% Analysis Date = 12/27/15 Pct Recovery = 96% Analysis Date = 12/27/15 Pct Recovery = 96% Analysis Date = 12/22/15 Pct Recovery = 96% Analysis Date = 12/22/15 Pct Recovery = 96% Analysis Date = 12/17/15 Pct Recovery = 96% Analysis Date = 12/17/15 Pct Recovery = 96% Analysis Date = 12/13/15 Pct Recovery = 96% Analysis Date = 12/13/15 Pct Recovery = 96% Analysis Date = 12/08/15 Pct Recovery = 96% Analysis Date = 12/08/15 Pct Recovery = 96% Analysis Date = 12/03/15 Pct Recovery = 96% Analysis Date = 12/03/15 Pct Recovery = 96% Analysis Date = 11/28/15 Pct Recovery = 96% Analysis Date = 11/28/15 Pct Recovery = 96% Analysis Date = 11/24/15 Pct Recovery = 96% Analysis Date = 11/24/15 Pct Recovery = 96% Analysis Date = 11/19/15 Pct Recovery = 96% Analysis Date = 11/19/15 Pct Recovery = 96% Analysis Date = 11/14/15 Pct Recovery = 96% Analysis Date = 11/14/15 Pct Recovery = 96% Analysis Date = 11/09/15 Pct Recovery = 96% Analysis Date = 11/09/15 Pct Recovery = 96% Analysis Date = 11/04/15 Pct Recovery = 96% Analysis Date = 11/04/15 Pct Recovery = 96% Analysis Date = 10/31/15 Pct Recovery = 96% Analysis Date = 10/31/15 Pct Recovery = 96% Analysis Date = 10/26/15 Pct Recovery = 95% Analysis Date = 10/26/15 Pct Recovery = 95% Analysis Date = 10/21/15 Pct Recovery = 95% Analysis Date = 10/21/15 Pct Recovery = 95% Analysis Date = 10/16/15 Pct Recovery = 95% Analysis Date = 10/16/15 Pct Recovery = 95% Analysis Date = 10/11/15 Pct Recovery = 95% Analysis Date = 10/11/15 Pct Recovery = 95% Analysis Date = 10/07/15 Pct Recovery = 94% Analysis Date = 10/07/15 Pct Recovery = 94% Analysis Date = 10/02/15 Pct Recovery = 94% Analysis Date = 10/02/15 Pct Recovery = 94% Analysis Date = 09/27/15 Pct Recovery = 94% Analysis Date = 09/27/15 Pct Recovery = 94% Analysis Date = 09/22/15 Pct Recovery = 94% Analysis Date = 09/22/15 Pct Recovery = 94% Analysis Date = 09/17/15 Pct Recovery = 93% Analysis Date = 09/17/15 Pct Recovery = 93% Analysis Date = 09/13/15 Pct Recovery = 93% Analysis Date = 09/13/15 Pct Recovery = 93% Analysis Date = 09/08/15 Pct Recovery = 93% Analysis Date = 09/08/15 Pct Recovery = 93% Analysis Date = 09/03/15 Pct Recovery = 93% Analysis Date = 09/03/15 Pct Recovery = 93% Analysis Date = 08/29/15 Pct Recovery = 92% Analysis Date = 08/29/15 Pct Recovery = 92% Analysis Date = 08/25/15 Pct Recovery = 92% Analysis Date = 08/25/15 Pct Recovery = 92% Analysis Date = 08/20/15 Pct Recovery = 92% Analysis Date = 08/20/15 Pct Recovery = 92% Analysis Date = 08/15/15 Pct Recovery = 92% Analysis Date = 08/15/15 Pct Recovery = 92% Analysis Date = 08/10/15 Pct Recovery = 91% Analysis Date = 08/10/15 Pct Recovery = 91% Analysis Date = 08/05/15 Pct Recovery = 91% Analysis Date = 08/05/15 Pct Recovery = 91% Analysis Date = 08/01/15 Pct Recovery = 91% Analysis Date = 08/01/15 Pct Recovery = 91% Analysis Date = 07/27/15 Pct Recovery = 91% Analysis Date = 07/27/15 Pct Recovery = 91% Analysis Date = 07/22/15 Pct Recovery = 90% Analysis Date = 07/22/15 Pct Recovery = 90% Analysis Date = 07/17/15 Pct Recovery = 90% Analysis Date = 07/17/15 Pct Recovery = 90% Analysis Date = 07/12/15 Pct Recovery = 90% Analysis Date = 07/12/15 Pct Recovery = 90% Analysis Date = 07/08/15 Pct Recovery = 90% Analysis Date = 07/08/15 Pct Recovery = 90% Analysis Date = 07/03/15 Pct Recovery = 89% Analysis Date = 07/03/15 Pct Recovery = 89% Analysis Date = 06/28/15 Pct Recovery = 89% Analysis Date = 06/28/15 Pct Recovery = 89% Analysis Date = 06/23/15 Pct Recovery = 89% Analysis Date = 06/23/15 Pct Recovery = 89% Analysis Date = 06/18/15 Pct Recovery = 89% Analysis Date = 06/18/15 Pct Recovery = 89% Analysis Date = 06/14/15 Pct Recovery = 88% Analysis Date = 06/14/15 Pct Recovery = 88% Analysis Date = 06/09/15 Pct Recovery = 88% Analysis Date = 06/09/15 Pct Recovery = 88% Analysis Date = 06/04/15 Pct Recovery = 88% Analysis Date = 06/04/15 Pct Recovery = 88% Analysis Date = 05/30/15 Pct Recovery = 88% Analysis Date = 05/30/15 Pct Recovery = 88% Analysis Date = 05/25/15 Pct Recovery = 87% Analysis Date = 05/25/15 Pct Recovery = 87% Analysis Date = 05/21/15 Pct Recovery = 87% Analysis Date = 05/21/15 Pct Recovery = 87% Analysis Date = 05/16/15 Pct Recovery = 87% Analysis Date = 05/16/15 Pct Recovery = 87% Analysis Date = 05/11/15 Pct Recovery = 87% Analysis Date = 05/11/15 Pct Recovery = 87% Analysis Date = 05/06/15 Pct Recovery = 86% Analysis Date = 05/06/15 Pct Recovery = 86% Analysis Date = 05/02/15 Pct Recovery = 86% Analysis Date = 05/02/15 Pct Recovery = 86% Analysis Date = 04/27/15 Pct Recovery = 86% Analysis Date = 04/27/15 Pct Recovery = 86% Analysis Date = 04/22/15 Pct Recovery = 86% Analysis Date = 04/22/15 Pct Recovery = 86% Analysis Date = 04/17/15 Pct Recovery = 86% Analysis Date = 04/17/15 Pct Recovery = 86% Analysis Date = 04/12/15 Pct Recovery = 85% Analysis Date = 04/12/15 Pct Recovery = 85% Analysis Date = 04/08/15 Pct Recovery = 85% Analysis Date = 04/08/15 Pct Recovery = 85% Analysis Date = 04/03/15 Pct Recovery = 85% Analysis Date = 04/03/15 Pct Recovery = 85% Analysis Date = 03/29/15 Pct Recovery = 85% Analysis Date = 03/29/15 Pct Recovery = 85% Analysis Date = 03/24/15 Pct Recovery = 84% Analysis Date = 03/24/15 Pct Recovery = 84% Analysis Date = 03/19/15 Pct Recovery = 84% Analysis Date = 03/19/15 Pct Recovery = 84% Analysis Date = 03/15/15 Pct Recovery = 84% Analysis Date = 03/15/15 Pct Recovery = 84% Analysis Date = 03/10/15 Pct Recovery = 84% Analysis Date = 03/10/15 Pct Recovery = 84% Analysis Date = 03/05/15 Pct Recovery = 84% Analysis Date = 03/05/15 Pct Recovery = 84% Analysis Date = 02/28/15 Pct Recovery = 83% Analysis Date = 02/28/15 Pct Recovery = 83% Analysis Date = 02/23/15 Pct Recovery = 83% Analysis Date = 02/23/15 Pct Recovery = 83% Analysis Date = 02/19/15 Pct Recovery = 83% Analysis Date = 02/19/15 Pct Recovery = 83% Analysis Date = 02/14/15 Pct Recovery = 83% Analysis Date = 02/14/15 Pct Recovery = 83% Analysis Date = 02/09/15 Pct Recovery = 83% Analysis Date = 02/09/15 Pct Recovery = 83% Analysis Date = 02/04/15 Pct Recovery = 82% Analysis Date = 02/04/15 Pct Recovery = 82% Analysis Date = 01/31/15 Pct Recovery = 82% Analysis Date = 01/31/15 Pct Recovery = 82% Analysis Date = 01/26/15 Pct Recovery = 82% Analysis Date = 01/26/15 Pct Recovery = 82% Analysis Date = 01/21/15 Pct Recovery = 82% Analysis Date = 01/21/15 Pct Recovery = 82% Analysis Date = 01/16/15 Pct Recovery = 81% Analysis Date = 01/16/15 Pct Recovery = 81% Analysis Date = 01/11/15 Pct Recovery = 81% Analysis Date = 01/11/15 Pct Recovery = 81% Analysis Date = 01/07/15 Pct Recovery = 81% Analysis Date = 01/07/15 Pct Recovery = 81% Analysis Date = 01/02/15 Pct Recovery = 81% Analysis Date = 01/02/15 Pct Recovery = 81% Analysis Date = 12/28/14 Pct Recovery = 81% Analysis Date = 12/28/14 Pct Recovery = 81% Analysis Date = 12/23/14 Pct Recovery = 80% Analysis Date = 12/23/14 Pct Recovery = 80% Analysis Date = 12/18/14 Pct Recovery = 80% Analysis Date = 12/18/14 Pct Recovery = 80% Analysis Date = 12/14/14 Pct Recovery = 80% Analysis Date = 12/14/14 Pct Recovery = 80% Analysis Date = 12/09/14 Pct Recovery = 80% Analysis Date = 12/09/14 Pct Recovery = 80% Analysis Date = 12/04/14 Pct Recovery = 79% Analysis Date = 12/04/14 Pct Recovery = 79% Analysis Date = 11/29/14 Pct Recovery = 79% Analysis Date = 11/29/14 Pct Recovery = 79% Analysis Date = 11/24/14 Pct Recovery = 79% Analysis Date = 11/24/14 Pct Recovery = 79% Analysis Date = 11/20/14 Pct Recovery = 79% Analysis Date = 11/20/14 Pct Recovery = 79% Analysis Date = 11/15/14 Pct Recovery = 79% Analysis Date = 11/15/14 Pct Recovery = 79% Analysis Date = 11/10/14 Pct Recovery = 79% Analysis Date = 11/10/14 Pct Recovery = 79% Analysis Date = 11/05/14 Pct Recovery = 79% Analysis Date = 11/05/14 Pct Recovery = 79% Analysis Date = 11/01/14 Pct Recovery = 79% Analysis Date = 11/01/14 Pct Recovery = 79% Analysis Date = 10/27/14 Pct Recovery = 78% Analysis Date = 10/27/14 Pct Recovery = 78% Analysis Date = 10/22/14 Pct Recovery = 78% Analysis Date = 10/22/14 Pct Recovery = 78% Analysis Date = 10/17/14 Pct Recovery = 78% Analysis Date = 10/17/14 Pct Recovery = 78% Analysis Date = 10/12/14 Pct Recovery = 78% Analysis Date = 10/12/14 Pct Recovery = 78% Analysis Date = 10/08/14 Pct Recovery = 78% Analysis Date = 10/08/14 Pct Recovery = 78% Analysis Date = 10/03/14 Pct Recovery = 78% Analysis Date = 10/03/14 Pct Recovery = 78% Analysis Date = 09/28/14 Pct Recovery = 78% Analysis Date = 09/28/14 Pct Recovery = 78% Analysis Date = 09/23/14 Pct Recovery = 78% Analysis Date = 09/23/14 Pct Recovery = 78% Analysis Date = 09/18/14 Pct Recovery = 78% Analysis Date = 09/18/14 Pct Recovery = 78% Analysis Date = 09/14/14 Pct Recovery = 78% Analysis Date = 09/14/14 Pct Recovery = 78% Analysis Date = 09/09/14 Pct Recovery = 78% Analysis Date = 09/09/14 Pct Recovery = 78% Analysis Date = 09/04/14 Pct Recovery = 78% Analysis Date = 09/04/14 Pct Recovery = 78% Analysis Date = 08/30/14 Pct Recovery = 77% Analysis Date = 08/30/14 Pct Recovery = 77% Analysis Date = 08/25/14 Pct Recovery = 77% Analysis Date = 08/25/14 Pct Recovery = 77% Analysis Date = 08/21/14 Pct Recovery = 77% Analysis Date = 08/21/14 Pct Recovery = 77% Analysis Date = 08/16/14 Pct Recovery = 77% Analysis Date = 08/16/14 Pct Recovery = 77% Analysis Date = 08/11/14 Pct Recovery = 77% Analysis Date = 08/11/14 Pct Recovery = 77% Analysis Date = 08/06/14 Pct Recovery = 77% Analysis Date = 08/06/14 Pct Recovery = 77% Analysis Date = 08/02/14 Pct Recovery = 77% Analysis Date = 08/02/14 Pct Recovery = 77% Analysis Date = 07/28/14 Pct Recovery = 77% Analysis Date = 07/28/14 Pct Recovery = 77% Analysis Date = 07/23/14 Pct Recovery = 77% Analysis Date = 07/23/14 Pct Recovery = 77% Analysis Date = 07/18/14 Pct Recovery = 77% Analysis Date = 07/18/14 Pct Recovery = 77% Analysis Date = 07/13/14 Pct Recovery = 77% Analysis Date = 07/13/14 Pct Recovery = 77% Analysis Date = 07/09/14 Pct Recovery = 77% Analysis Date = 07/09/14 Pct Recovery = 77% Analysis Date = 07/04/14 Pct Recovery = 77% Analysis Date = 07/04/14 Pct Recovery = 77% Analysis Date = 06/29/14 Pct Recovery = 77% Analysis Date = 06/29/14 Pct Recovery = 77% Analysis Date = 06/24/14 Pct Recovery = 76% Analysis Date = 06/24/14 Pct Recovery = 76% Analysis Date = 06/19/14 Pct Recovery = 76% Analysis Date = 06/19/14 Pct Recovery = 76% Analysis Date = 06/15/14 Pct Recovery = 76% Analysis Date = 06/15/14 Pct Recovery = 76% Analysis Date = 06/10/14 Pct Recovery = 76% Analysis Date = 06/10/14 Pct Recovery = 76% Analysis Date = 06/05/14 Pct Recovery = 76% Analysis Date = 06/05/14 Pct Recovery = 76% Analysis Date = 05/31/14 Pct Recovery = 76% Analysis Date = 05/31/14 Pct Recovery = 76% Analysis Date = 05/26/14 Pct Recovery = 76% Analysis Date = 05/26/14 Pct Recovery = 76% Analysis Date = 05/22/14 Pct Recovery = 76% Analysis Date = 05/22/14 Pct Recovery = 76% Analysis Date = 05/17/14 Pct Recovery = 76% Analysis Date = 05/17/14 Pct Recovery = 76% Analysis Date = 05/12/14 Pct Recovery = 76% Analysis Date = 05/12/14 Pct Recovery = 76% Analysis Date = 05/07/14 Pct Recovery = 76% Analysis Date = 05/07/14 Pct Recovery = 76% Analysis Date = 05/03/14 Pct Recovery = 76% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
CIS-1,3-DICHLOROPROPENE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 50 87% 21% 91% 22%
Total 50 87% 21% 91% 22%

Sample Statistics
CIS-1,3-DICHLOROPROPENE

Characteristic N % % Basis
Plotted 50 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 50 .  
False Negatives 0 0% 0 out of 50
Not Spiked 23 .  
False Positives 0 0% 0 out of 23

BQS OBSP Determination:
DIBROMOCHLOROMETHANE
METHOD: 4440 , TESTIDCODE: 32105GCM66
Open Data Set

Analysis Date = 12/16/16 SpikeMix = NSI 041816AVOC: 40 µl & ChemService 5082900: 40 µl Pct Recovery = 110% Analysis Date = 07/14/16 SpikeMix = Accu 216041125: 40 µl & NSI 041816AVOC: 40 µl Pct Recovery = 110% Analysis Date = 08/26/16 SpikeMix = NSI 041816AVOC: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 113% Analysis Date = 11/22/14 SpikeMix = NSI 032614: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 89% Analysis Date = 06/10/14 SpikeMix = Crescent 03DD004: 20 µl & NSI 032614: 20 µl Pct Recovery = 87% Analysis Date = 06/10/14 SpikeMix = NSI 032614: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 92% Analysis Date = 05/01/14 SpikeMix = Accu 214031115: 20 µl & NSI 032614: 20 µl Pct Recovery = 85% Analysis Date = 04/09/15 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 91% Analysis Date = 03/06/15 SpikeMix = ERA 0227-14-06.1A: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 87% Analysis Date = 11/14/14 SpikeMix = Crescent 03DD004: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 90% Analysis Date = 08/16/14 SpikeMix = ERA 0227-14-06.1A: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 93% Analysis Date = 07/01/14 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 93% Analysis Date = 08/15/15 SpikeMix = Supelco LC13545: 25 µl & Crescent 04EE008: 25 µl Pct Recovery = 105% Analysis Date = 06/16/15 SpikeMix = ERA 0406-15-03: 25 µl & Supelco LC13545: 25 µl Pct Recovery = 90% Analysis Date = 10/13/16 SpikeMix = Accu 216041125: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 116% Analysis Date = 10/13/16 SpikeMix = NSI 041816AVOC: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 109% Analysis Date = 07/29/16 SpikeMix = Phenova B20160319: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 121% Analysis Date = 06/10/16 SpikeMix = NSI 041816AVOC: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 93% Analysis Date = 04/02/16 SpikeMix = Supelco LC13545: 15 µl & Accu 215041380: 15 µl Pct Recovery = 99% Analysis Date = 12/18/15 SpikeMix = Supelco LC13545: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 90% Analysis Date = 04/26/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 104% Analysis Date = 02/05/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 77% Analysis Date = 11/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 96% Analysis Date = 10/16/15 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 96% Analysis Date = 05/09/15 SpikeMix = Spex Organics EN150428007: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 91% Analysis Date = 09/09/14 SpikeMix = Accu 214031115: 10 µl & NSI 032614: 10 µl Pct Recovery = 100% Analysis Date = 09/09/14 SpikeMix = NSI 032614: 10 µl & Spex Organics C1140417015: 10 µl Pct Recovery = 97% Analysis Date = 07/29/14 SpikeMix = Crescent 03DD004: 10 µl & NSI 032614: 10 µl Pct Recovery = 104% Analysis Date = 05/30/14 SpikeMix = NSI 032614: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 98% Analysis Date = 01/13/15 SpikeMix = Accu 214031115: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 88% Analysis Date = 10/21/14 SpikeMix = ERA 0227-14-06.1A: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 94% Analysis Date = 10/04/14 SpikeMix = Crescent 03DD004: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 100% Analysis Date = 07/11/14 SpikeMix = Spex Organics C1140417015: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 95% Analysis Date = 05/13/16 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 107% Analysis Date = 03/17/16 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 108% Analysis Date = 12/10/15 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 100% Analysis Date = 06/27/15 SpikeMix = ERA 0406-15-03: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 98% Analysis Date = 05/09/15 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 94% Analysis Date = 02/18/16 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 99% Analysis Date = 11/12/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 90% Analysis Date = 09/03/15 SpikeMix = NSI 050515AVOC: 10 µl & Spex Organics EN150428007: 10 µl Pct Recovery = 109% Analysis Date = 05/21/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 92% Analysis Date = 12/15/16 Pct Recovery = 116% Analysis Date = 12/11/16 Pct Recovery = 115% Analysis Date = 12/11/16 Pct Recovery = 115% Analysis Date = 12/06/16 Pct Recovery = 115% Analysis Date = 12/06/16 Pct Recovery = 115% Analysis Date = 12/01/16 Pct Recovery = 115% Analysis Date = 12/01/16 Pct Recovery = 115% Analysis Date = 11/26/16 Pct Recovery = 115% Analysis Date = 11/26/16 Pct Recovery = 115% Analysis Date = 11/21/16 Pct Recovery = 114% Analysis Date = 11/21/16 Pct Recovery = 114% Analysis Date = 11/17/16 Pct Recovery = 114% Analysis Date = 11/17/16 Pct Recovery = 114% Analysis Date = 11/12/16 Pct Recovery = 114% Analysis Date = 11/12/16 Pct Recovery = 114% Analysis Date = 11/07/16 Pct Recovery = 114% Analysis Date = 11/07/16 Pct Recovery = 114% Analysis Date = 11/02/16 Pct Recovery = 113% Analysis Date = 11/02/16 Pct Recovery = 113% Analysis Date = 10/28/16 Pct Recovery = 113% Analysis Date = 10/28/16 Pct Recovery = 113% Analysis Date = 10/24/16 Pct Recovery = 113% Analysis Date = 10/24/16 Pct Recovery = 113% Analysis Date = 10/19/16 Pct Recovery = 112% Analysis Date = 10/19/16 Pct Recovery = 112% Analysis Date = 10/14/16 Pct Recovery = 112% Analysis Date = 10/14/16 Pct Recovery = 112% Analysis Date = 10/09/16 Pct Recovery = 112% Analysis Date = 10/09/16 Pct Recovery = 112% Analysis Date = 10/04/16 Pct Recovery = 112% Analysis Date = 10/04/16 Pct Recovery = 112% Analysis Date = 09/30/16 Pct Recovery = 111% Analysis Date = 09/30/16 Pct Recovery = 111% Analysis Date = 09/25/16 Pct Recovery = 111% Analysis Date = 09/25/16 Pct Recovery = 111% Analysis Date = 09/20/16 Pct Recovery = 111% Analysis Date = 09/20/16 Pct Recovery = 111% Analysis Date = 09/15/16 Pct Recovery = 111% Analysis Date = 09/15/16 Pct Recovery = 111% Analysis Date = 09/10/16 Pct Recovery = 110% Analysis Date = 09/10/16 Pct Recovery = 110% Analysis Date = 09/06/16 Pct Recovery = 110% Analysis Date = 09/06/16 Pct Recovery = 110% Analysis Date = 09/01/16 Pct Recovery = 110% Analysis Date = 09/01/16 Pct Recovery = 110% Analysis Date = 08/27/16 Pct Recovery = 110% Analysis Date = 08/27/16 Pct Recovery = 110% Analysis Date = 08/22/16 Pct Recovery = 109% Analysis Date = 08/22/16 Pct Recovery = 109% Analysis Date = 08/17/16 Pct Recovery = 109% Analysis Date = 08/17/16 Pct Recovery = 109% Analysis Date = 08/13/16 Pct Recovery = 109% Analysis Date = 08/13/16 Pct Recovery = 109% Analysis Date = 08/08/16 Pct Recovery = 108% Analysis Date = 08/08/16 Pct Recovery = 108% Analysis Date = 08/03/16 Pct Recovery = 108% Analysis Date = 08/03/16 Pct Recovery = 108% Analysis Date = 07/29/16 Pct Recovery = 108% Analysis Date = 07/29/16 Pct Recovery = 108% Analysis Date = 07/24/16 Pct Recovery = 108% Analysis Date = 07/24/16 Pct Recovery = 108% Analysis Date = 07/20/16 Pct Recovery = 107% Analysis Date = 07/20/16 Pct Recovery = 107% Analysis Date = 07/15/16 Pct Recovery = 107% Analysis Date = 07/15/16 Pct Recovery = 107% Analysis Date = 07/10/16 Pct Recovery = 107% Analysis Date = 07/10/16 Pct Recovery = 107% Analysis Date = 07/05/16 Pct Recovery = 107% Analysis Date = 07/05/16 Pct Recovery = 107% Analysis Date = 06/30/16 Pct Recovery = 106% Analysis Date = 06/30/16 Pct Recovery = 106% Analysis Date = 06/26/16 Pct Recovery = 106% Analysis Date = 06/26/16 Pct Recovery = 106% Analysis Date = 06/21/16 Pct Recovery = 106% Analysis Date = 06/21/16 Pct Recovery = 106% Analysis Date = 06/16/16 Pct Recovery = 106% Analysis Date = 06/16/16 Pct Recovery = 106% Analysis Date = 06/11/16 Pct Recovery = 105% Analysis Date = 06/11/16 Pct Recovery = 105% Analysis Date = 06/06/16 Pct Recovery = 105% Analysis Date = 06/06/16 Pct Recovery = 105% Analysis Date = 06/02/16 Pct Recovery = 105% Analysis Date = 06/02/16 Pct Recovery = 105% Analysis Date = 05/28/16 Pct Recovery = 105% Analysis Date = 05/28/16 Pct Recovery = 105% Analysis Date = 05/23/16 Pct Recovery = 104% Analysis Date = 05/23/16 Pct Recovery = 104% Analysis Date = 05/18/16 Pct Recovery = 104% Analysis Date = 05/18/16 Pct Recovery = 104% Analysis Date = 05/13/16 Pct Recovery = 104% Analysis Date = 05/13/16 Pct Recovery = 104% Analysis Date = 05/09/16 Pct Recovery = 104% Analysis Date = 05/09/16 Pct Recovery = 104% Analysis Date = 05/04/16 Pct Recovery = 103% Analysis Date = 05/04/16 Pct Recovery = 103% Analysis Date = 04/29/16 Pct Recovery = 103% Analysis Date = 04/29/16 Pct Recovery = 103% Analysis Date = 04/24/16 Pct Recovery = 103% Analysis Date = 04/24/16 Pct Recovery = 103% Analysis Date = 04/19/16 Pct Recovery = 103% Analysis Date = 04/19/16 Pct Recovery = 103% Analysis Date = 04/15/16 Pct Recovery = 102% Analysis Date = 04/15/16 Pct Recovery = 102% Analysis Date = 04/10/16 Pct Recovery = 102% Analysis Date = 04/10/16 Pct Recovery = 102% Analysis Date = 04/05/16 Pct Recovery = 102% Analysis Date = 04/05/16 Pct Recovery = 102% Analysis Date = 03/31/16 Pct Recovery = 102% Analysis Date = 03/31/16 Pct Recovery = 102% Analysis Date = 03/26/16 Pct Recovery = 101% Analysis Date = 03/26/16 Pct Recovery = 101% Analysis Date = 03/22/16 Pct Recovery = 101% Analysis Date = 03/22/16 Pct Recovery = 101% Analysis Date = 03/17/16 Pct Recovery = 101% Analysis Date = 03/17/16 Pct Recovery = 101% Analysis Date = 03/12/16 Pct Recovery = 101% Analysis Date = 03/12/16 Pct Recovery = 101% Analysis Date = 03/07/16 Pct Recovery = 101% Analysis Date = 03/07/16 Pct Recovery = 101% Analysis Date = 03/02/16 Pct Recovery = 100% Analysis Date = 03/02/16 Pct Recovery = 100% Analysis Date = 02/27/16 Pct Recovery = 100% Analysis Date = 02/27/16 Pct Recovery = 100% Analysis Date = 02/22/16 Pct Recovery = 100% Analysis Date = 02/22/16 Pct Recovery = 100% Analysis Date = 02/17/16 Pct Recovery = 100% Analysis Date = 02/17/16 Pct Recovery = 100% Analysis Date = 02/12/16 Pct Recovery = 100% Analysis Date = 02/12/16 Pct Recovery = 100% Analysis Date = 02/07/16 Pct Recovery = 100% Analysis Date = 02/07/16 Pct Recovery = 100% Analysis Date = 02/03/16 Pct Recovery = 100% Analysis Date = 02/03/16 Pct Recovery = 100% Analysis Date = 01/29/16 Pct Recovery = 99% Analysis Date = 01/29/16 Pct Recovery = 99% Analysis Date = 01/24/16 Pct Recovery = 99% Analysis Date = 01/24/16 Pct Recovery = 99% Analysis Date = 01/19/16 Pct Recovery = 99% Analysis Date = 01/19/16 Pct Recovery = 99% Analysis Date = 01/14/16 Pct Recovery = 99% Analysis Date = 01/14/16 Pct Recovery = 99% Analysis Date = 01/10/16 Pct Recovery = 99% Analysis Date = 01/10/16 Pct Recovery = 99% Analysis Date = 01/05/16 Pct Recovery = 99% Analysis Date = 01/05/16 Pct Recovery = 99% Analysis Date = 12/31/15 Pct Recovery = 98% Analysis Date = 12/31/15 Pct Recovery = 98% Analysis Date = 12/26/15 Pct Recovery = 98% Analysis Date = 12/26/15 Pct Recovery = 98% Analysis Date = 12/21/15 Pct Recovery = 98% Analysis Date = 12/21/15 Pct Recovery = 98% Analysis Date = 12/17/15 Pct Recovery = 98% Analysis Date = 12/17/15 Pct Recovery = 98% Analysis Date = 12/12/15 Pct Recovery = 98% Analysis Date = 12/12/15 Pct Recovery = 98% Analysis Date = 12/07/15 Pct Recovery = 98% Analysis Date = 12/07/15 Pct Recovery = 98% Analysis Date = 12/02/15 Pct Recovery = 97% Analysis Date = 12/02/15 Pct Recovery = 97% Analysis Date = 11/27/15 Pct Recovery = 97% Analysis Date = 11/27/15 Pct Recovery = 97% Analysis Date = 11/23/15 Pct Recovery = 97% Analysis Date = 11/23/15 Pct Recovery = 97% Analysis Date = 11/18/15 Pct Recovery = 97% Analysis Date = 11/18/15 Pct Recovery = 97% Analysis Date = 11/13/15 Pct Recovery = 97% Analysis Date = 11/13/15 Pct Recovery = 97% Analysis Date = 11/08/15 Pct Recovery = 97% Analysis Date = 11/08/15 Pct Recovery = 97% Analysis Date = 11/03/15 Pct Recovery = 97% Analysis Date = 11/03/15 Pct Recovery = 97% Analysis Date = 10/30/15 Pct Recovery = 96% Analysis Date = 10/30/15 Pct Recovery = 96% Analysis Date = 10/25/15 Pct Recovery = 96% Analysis Date = 10/25/15 Pct Recovery = 96% Analysis Date = 10/20/15 Pct Recovery = 96% Analysis Date = 10/20/15 Pct Recovery = 96% Analysis Date = 10/15/15 Pct Recovery = 96% Analysis Date = 10/15/15 Pct Recovery = 96% Analysis Date = 10/10/15 Pct Recovery = 96% Analysis Date = 10/10/15 Pct Recovery = 96% Analysis Date = 10/06/15 Pct Recovery = 96% Analysis Date = 10/06/15 Pct Recovery = 96% Analysis Date = 10/01/15 Pct Recovery = 96% Analysis Date = 10/01/15 Pct Recovery = 96% Analysis Date = 09/26/15 Pct Recovery = 96% Analysis Date = 09/26/15 Pct Recovery = 96% Analysis Date = 09/21/15 Pct Recovery = 96% Analysis Date = 09/21/15 Pct Recovery = 96% Analysis Date = 09/16/15 Pct Recovery = 96% Analysis Date = 09/16/15 Pct Recovery = 96% Analysis Date = 09/12/15 Pct Recovery = 95% Analysis Date = 09/12/15 Pct Recovery = 95% Analysis Date = 09/07/15 Pct Recovery = 95% Analysis Date = 09/07/15 Pct Recovery = 95% Analysis Date = 09/02/15 Pct Recovery = 95% Analysis Date = 09/02/15 Pct Recovery = 95% Analysis Date = 08/28/15 Pct Recovery = 95% Analysis Date = 08/28/15 Pct Recovery = 95% Analysis Date = 08/23/15 Pct Recovery = 95% Analysis Date = 08/23/15 Pct Recovery = 95% Analysis Date = 08/19/15 Pct Recovery = 95% Analysis Date = 08/19/15 Pct Recovery = 95% Analysis Date = 08/14/15 Pct Recovery = 95% Analysis Date = 08/14/15 Pct Recovery = 95% Analysis Date = 08/09/15 Pct Recovery = 95% Analysis Date = 08/09/15 Pct Recovery = 95% Analysis Date = 08/04/15 Pct Recovery = 95% Analysis Date = 08/04/15 Pct Recovery = 95% Analysis Date = 07/30/15 Pct Recovery = 95% Analysis Date = 07/30/15 Pct Recovery = 95% Analysis Date = 07/26/15 Pct Recovery = 95% Analysis Date = 07/26/15 Pct Recovery = 95% Analysis Date = 07/21/15 Pct Recovery = 95% Analysis Date = 07/21/15 Pct Recovery = 95% Analysis Date = 07/16/15 Pct Recovery = 95% Analysis Date = 07/16/15 Pct Recovery = 95% Analysis Date = 07/11/15 Pct Recovery = 94% Analysis Date = 07/11/15 Pct Recovery = 94% Analysis Date = 07/06/15 Pct Recovery = 94% Analysis Date = 07/06/15 Pct Recovery = 94% Analysis Date = 07/02/15 Pct Recovery = 94% Analysis Date = 07/02/15 Pct Recovery = 94% Analysis Date = 06/27/15 Pct Recovery = 94% Analysis Date = 06/27/15 Pct Recovery = 94% Analysis Date = 06/22/15 Pct Recovery = 94% Analysis Date = 06/22/15 Pct Recovery = 94% Analysis Date = 06/17/15 Pct Recovery = 94% Analysis Date = 06/17/15 Pct Recovery = 94% Analysis Date = 06/12/15 Pct Recovery = 94% Analysis Date = 06/12/15 Pct Recovery = 94% Analysis Date = 06/08/15 Pct Recovery = 94% Analysis Date = 06/08/15 Pct Recovery = 94% Analysis Date = 06/03/15 Pct Recovery = 94% Analysis Date = 06/03/15 Pct Recovery = 94% Analysis Date = 05/29/15 Pct Recovery = 94% Analysis Date = 05/29/15 Pct Recovery = 94% Analysis Date = 05/24/15 Pct Recovery = 94% Analysis Date = 05/24/15 Pct Recovery = 94% Analysis Date = 05/19/15 Pct Recovery = 94% Analysis Date = 05/19/15 Pct Recovery = 94% Analysis Date = 05/15/15 Pct Recovery = 94% Analysis Date = 05/15/15 Pct Recovery = 94% Analysis Date = 05/10/15 Pct Recovery = 94% Analysis Date = 05/10/15 Pct Recovery = 94% Analysis Date = 05/05/15 Pct Recovery = 94% Analysis Date = 05/05/15 Pct Recovery = 94% Analysis Date = 04/30/15 Pct Recovery = 94% Analysis Date = 04/30/15 Pct Recovery = 94% Analysis Date = 04/25/15 Pct Recovery = 94% Analysis Date = 04/25/15 Pct Recovery = 94% Analysis Date = 04/21/15 Pct Recovery = 94% Analysis Date = 04/21/15 Pct Recovery = 94% Analysis Date = 04/16/15 Pct Recovery = 94% Analysis Date = 04/16/15 Pct Recovery = 94% Analysis Date = 04/11/15 Pct Recovery = 94% Analysis Date = 04/11/15 Pct Recovery = 94% Analysis Date = 04/06/15 Pct Recovery = 93% Analysis Date = 04/06/15 Pct Recovery = 93% Analysis Date = 04/01/15 Pct Recovery = 93% Analysis Date = 04/01/15 Pct Recovery = 93% Analysis Date = 03/28/15 Pct Recovery = 93% Analysis Date = 03/28/15 Pct Recovery = 93% Analysis Date = 03/23/15 Pct Recovery = 93% Analysis Date = 03/23/15 Pct Recovery = 93% Analysis Date = 03/18/15 Pct Recovery = 93% Analysis Date = 03/18/15 Pct Recovery = 93% Analysis Date = 03/13/15 Pct Recovery = 93% Analysis Date = 03/13/15 Pct Recovery = 93% Analysis Date = 03/08/15 Pct Recovery = 93% Analysis Date = 03/08/15 Pct Recovery = 93% Analysis Date = 03/04/15 Pct Recovery = 93% Analysis Date = 03/04/15 Pct Recovery = 93% Analysis Date = 02/27/15 Pct Recovery = 93% Analysis Date = 02/27/15 Pct Recovery = 93% Analysis Date = 02/22/15 Pct Recovery = 93% Analysis Date = 02/22/15 Pct Recovery = 93% Analysis Date = 02/17/15 Pct Recovery = 93% Analysis Date = 02/17/15 Pct Recovery = 93% Analysis Date = 02/12/15 Pct Recovery = 93% Analysis Date = 02/12/15 Pct Recovery = 93% Analysis Date = 02/08/15 Pct Recovery = 93% Analysis Date = 02/08/15 Pct Recovery = 93% Analysis Date = 02/03/15 Pct Recovery = 93% Analysis Date = 02/03/15 Pct Recovery = 93% Analysis Date = 01/29/15 Pct Recovery = 93% Analysis Date = 01/29/15 Pct Recovery = 93% Analysis Date = 01/24/15 Pct Recovery = 93% Analysis Date = 01/24/15 Pct Recovery = 93% Analysis Date = 01/19/15 Pct Recovery = 93% Analysis Date = 01/19/15 Pct Recovery = 93% Analysis Date = 01/15/15 Pct Recovery = 93% Analysis Date = 01/15/15 Pct Recovery = 93% Analysis Date = 01/10/15 Pct Recovery = 93% Analysis Date = 01/10/15 Pct Recovery = 93% Analysis Date = 01/05/15 Pct Recovery = 93% Analysis Date = 01/05/15 Pct Recovery = 93% Analysis Date = 12/31/14 Pct Recovery = 93% Analysis Date = 12/31/14 Pct Recovery = 93% Analysis Date = 12/26/14 Pct Recovery = 93% Analysis Date = 12/26/14 Pct Recovery = 93% Analysis Date = 12/22/14 Pct Recovery = 93% Analysis Date = 12/22/14 Pct Recovery = 93% Analysis Date = 12/17/14 Pct Recovery = 93% Analysis Date = 12/17/14 Pct Recovery = 93% Analysis Date = 12/12/14 Pct Recovery = 93% Analysis Date = 12/12/14 Pct Recovery = 93% Analysis Date = 12/07/14 Pct Recovery = 93% Analysis Date = 12/07/14 Pct Recovery = 93% Analysis Date = 12/02/14 Pct Recovery = 93% Analysis Date = 12/02/14 Pct Recovery = 93% Analysis Date = 11/28/14 Pct Recovery = 93% Analysis Date = 11/28/14 Pct Recovery = 93% Analysis Date = 11/23/14 Pct Recovery = 93% Analysis Date = 11/23/14 Pct Recovery = 93% Analysis Date = 11/18/14 Pct Recovery = 93% Analysis Date = 11/18/14 Pct Recovery = 93% Analysis Date = 11/13/14 Pct Recovery = 93% Analysis Date = 11/13/14 Pct Recovery = 93% Analysis Date = 11/08/14 Pct Recovery = 93% Analysis Date = 11/08/14 Pct Recovery = 93% Analysis Date = 11/04/14 Pct Recovery = 93% Analysis Date = 11/04/14 Pct Recovery = 93% Analysis Date = 10/30/14 Pct Recovery = 93% Analysis Date = 10/30/14 Pct Recovery = 93% Analysis Date = 10/25/14 Pct Recovery = 93% Analysis Date = 10/25/14 Pct Recovery = 93% Analysis Date = 10/20/14 Pct Recovery = 93% Analysis Date = 10/20/14 Pct Recovery = 93% Analysis Date = 10/15/14 Pct Recovery = 93% Analysis Date = 10/15/14 Pct Recovery = 93% Analysis Date = 10/11/14 Pct Recovery = 93% Analysis Date = 10/11/14 Pct Recovery = 93% Analysis Date = 10/06/14 Pct Recovery = 93% Analysis Date = 10/06/14 Pct Recovery = 93% Analysis Date = 10/01/14 Pct Recovery = 93% Analysis Date = 10/01/14 Pct Recovery = 93% Analysis Date = 09/26/14 Pct Recovery = 93% Analysis Date = 09/26/14 Pct Recovery = 93% Analysis Date = 09/21/14 Pct Recovery = 93% Analysis Date = 09/21/14 Pct Recovery = 93% Analysis Date = 09/17/14 Pct Recovery = 93% Analysis Date = 09/17/14 Pct Recovery = 93% Analysis Date = 09/12/14 Pct Recovery = 93% Analysis Date = 09/12/14 Pct Recovery = 93% Analysis Date = 09/07/14 Pct Recovery = 93% Analysis Date = 09/07/14 Pct Recovery = 93% Analysis Date = 09/02/14 Pct Recovery = 93% Analysis Date = 09/02/14 Pct Recovery = 93% Analysis Date = 08/28/14 Pct Recovery = 94% Analysis Date = 08/28/14 Pct Recovery = 94% Analysis Date = 08/24/14 Pct Recovery = 94% Analysis Date = 08/24/14 Pct Recovery = 94% Analysis Date = 08/19/14 Pct Recovery = 94% Analysis Date = 08/19/14 Pct Recovery = 94% Analysis Date = 08/14/14 Pct Recovery = 94% Analysis Date = 08/14/14 Pct Recovery = 94% Analysis Date = 08/09/14 Pct Recovery = 94% Analysis Date = 08/09/14 Pct Recovery = 94% Analysis Date = 08/04/14 Pct Recovery = 94% Analysis Date = 08/04/14 Pct Recovery = 94% Analysis Date = 07/31/14 Pct Recovery = 94% Analysis Date = 07/31/14 Pct Recovery = 94% Analysis Date = 07/26/14 Pct Recovery = 94% Analysis Date = 07/26/14 Pct Recovery = 94% Analysis Date = 07/21/14 Pct Recovery = 94% Analysis Date = 07/21/14 Pct Recovery = 94% Analysis Date = 07/16/14 Pct Recovery = 94% Analysis Date = 07/16/14 Pct Recovery = 94% Analysis Date = 07/11/14 Pct Recovery = 94% Analysis Date = 07/11/14 Pct Recovery = 94% Analysis Date = 07/07/14 Pct Recovery = 94% Analysis Date = 07/07/14 Pct Recovery = 94% Analysis Date = 07/02/14 Pct Recovery = 94% Analysis Date = 07/02/14 Pct Recovery = 94% Analysis Date = 06/27/14 Pct Recovery = 94% Analysis Date = 06/27/14 Pct Recovery = 94% Analysis Date = 06/22/14 Pct Recovery = 94% Analysis Date = 06/22/14 Pct Recovery = 94% Analysis Date = 06/17/14 Pct Recovery = 94% Analysis Date = 06/17/14 Pct Recovery = 94% Analysis Date = 06/13/14 Pct Recovery = 94% Analysis Date = 06/13/14 Pct Recovery = 94% Analysis Date = 06/08/14 Pct Recovery = 94% Analysis Date = 06/08/14 Pct Recovery = 94% Analysis Date = 06/03/14 Pct Recovery = 94% Analysis Date = 06/03/14 Pct Recovery = 94% Analysis Date = 05/29/14 Pct Recovery = 94% Analysis Date = 05/29/14 Pct Recovery = 94% Analysis Date = 05/24/14 Pct Recovery = 94% Analysis Date = 05/24/14 Pct Recovery = 94% Analysis Date = 05/20/14 Pct Recovery = 94% Analysis Date = 05/20/14 Pct Recovery = 94% Analysis Date = 05/15/14 Pct Recovery = 94% Analysis Date = 05/15/14 Pct Recovery = 94% Analysis Date = 05/10/14 Pct Recovery = 94% Analysis Date = 05/10/14 Pct Recovery = 94% Analysis Date = 05/05/14 Pct Recovery = 94% Analysis Date = 05/05/14 Pct Recovery = 94% Analysis Date = 05/01/14 Pct Recovery = 94% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
DIBROMOCHLOROMETHANE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 42 98% 9% 96% 10%
Total 42 98% 9% 96% 10%

Sample Statistics
DIBROMOCHLOROMETHANE

Characteristic N % % Basis
Plotted 42 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 42 .  
False Negatives 0 0% 0 out of 42
Not Spiked 22 .  
False Positives 0 0% 0 out of 22

BQS OBSP Determination:
DIBROMOMETHANE
METHOD: 4440 , TESTIDCODE: 30217GCM66
Open Data Set

Analysis Date = 12/12/16 SpikeMix = Accu 216041125: 40 µl & Crescent 03FF058: 40 µl Pct Recovery = 99% Analysis Date = 08/04/16 SpikeMix = Crescent 03FF058: 40 µl & Supelco LC20141V: 40 µl Pct Recovery = 90% Analysis Date = 04/09/15 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 105% Analysis Date = 03/06/15 SpikeMix = ERA 0227-14-06.1A: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 97% Analysis Date = 11/14/14 SpikeMix = Crescent 03DD004: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 95% Analysis Date = 08/16/14 SpikeMix = ERA 0227-14-06.1A: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 100% Analysis Date = 07/01/14 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 112% Analysis Date = 11/21/16 SpikeMix = Crescent 03FF058: 25 µl & Supelco LC20141V: 25 µl Pct Recovery = 97% Analysis Date = 06/30/16 SpikeMix = Crescent 03FF058: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 92% Analysis Date = 06/21/16 SpikeMix = Phenova B20160319: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 96% Analysis Date = 05/24/16 SpikeMix = Accu 216041125: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 90% Analysis Date = 11/22/14 SpikeMix = NSI 032614: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 98% Analysis Date = 06/10/14 SpikeMix = Crescent 03DD004: 20 µl & NSI 032614: 20 µl Pct Recovery = 109% Analysis Date = 06/10/14 SpikeMix = NSI 032614: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 109% Analysis Date = 05/01/14 SpikeMix = Accu 214031115: 20 µl & NSI 032614: 20 µl Pct Recovery = 103% Analysis Date = 09/29/15 SpikeMix = Accu 215041380: 25 µl & ERA 0406-15-03: 25 µl Pct Recovery = 89% Analysis Date = 08/15/15 SpikeMix = Supelco LC13545: 25 µl & Crescent 04EE008: 25 µl Pct Recovery = 94% Analysis Date = 07/13/15 SpikeMix = Crescent 04EE008: 25 µl & NSI 050515AVOC: 25 µl Pct Recovery = 97% Analysis Date = 09/28/16 SpikeMix = Crescent 03FF058: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 100% Analysis Date = 09/08/16 SpikeMix = Phenova B20160319: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 105% Analysis Date = 08/20/16 SpikeMix = Accu 216041125: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 104% Analysis Date = 04/02/16 SpikeMix = Supelco LC13545: 15 µl & Accu 215041380: 15 µl Pct Recovery = 91% Analysis Date = 03/04/16 SpikeMix = Accu 215041380: 15 µl & ERA 0406-15-03: 15 µl Pct Recovery = 88% Analysis Date = 06/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Accu 215041380: 15 µl Pct Recovery = 78% Analysis Date = 12/18/15 SpikeMix = Supelco LC13545: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 100% Analysis Date = 10/17/15 SpikeMix = Crescent 04EE008: 15 µl & NSI 050515AVOC: 15 µl Pct Recovery = 96% Analysis Date = 05/09/15 SpikeMix = Spex Organics EN150428007: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 98% Analysis Date = 01/13/15 SpikeMix = Accu 214031115: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 90% Analysis Date = 10/21/14 SpikeMix = ERA 0227-14-06.1A: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 95% Analysis Date = 10/04/14 SpikeMix = Crescent 03DD004: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 103% Analysis Date = 07/11/14 SpikeMix = Spex Organics C1140417015: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 104% Analysis Date = 09/09/14 SpikeMix = Accu 214031115: 10 µl & NSI 032614: 10 µl Pct Recovery = 122% Analysis Date = 09/09/14 SpikeMix = NSI 032614: 10 µl & Spex Organics C1140417015: 10 µl Pct Recovery = 108% Analysis Date = 07/29/14 SpikeMix = Crescent 03DD004: 10 µl & NSI 032614: 10 µl Pct Recovery = 108% Analysis Date = 05/30/14 SpikeMix = NSI 032614: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 89% Analysis Date = 02/18/16 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 95% Analysis Date = 11/20/15 SpikeMix = Accu 215041380: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 94% Analysis Date = 11/12/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 93% Analysis Date = 05/21/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 89% Analysis Date = 05/13/16 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 108% Analysis Date = 01/27/16 SpikeMix = Crescent 04EE008: 10 µl & NSI 050515AVOC: 10 µl Pct Recovery = 98% Analysis Date = 07/31/15 SpikeMix = Crescent 04EE008: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 84% Analysis Date = 05/09/15 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 95% Analysis Date = 12/11/16 Pct Recovery = 99% Analysis Date = 12/07/16 Pct Recovery = 99% Analysis Date = 12/07/16 Pct Recovery = 99% Analysis Date = 12/02/16 Pct Recovery = 99% Analysis Date = 12/02/16 Pct Recovery = 99% Analysis Date = 11/27/16 Pct Recovery = 99% Analysis Date = 11/27/16 Pct Recovery = 99% Analysis Date = 11/22/16 Pct Recovery = 99% Analysis Date = 11/22/16 Pct Recovery = 99% Analysis Date = 11/18/16 Pct Recovery = 99% Analysis Date = 11/18/16 Pct Recovery = 99% Analysis Date = 11/13/16 Pct Recovery = 99% Analysis Date = 11/13/16 Pct Recovery = 99% Analysis Date = 11/08/16 Pct Recovery = 99% Analysis Date = 11/08/16 Pct Recovery = 99% Analysis Date = 11/03/16 Pct Recovery = 99% Analysis Date = 11/03/16 Pct Recovery = 99% Analysis Date = 10/29/16 Pct Recovery = 99% Analysis Date = 10/29/16 Pct Recovery = 99% Analysis Date = 10/25/16 Pct Recovery = 99% Analysis Date = 10/25/16 Pct Recovery = 99% Analysis Date = 10/20/16 Pct Recovery = 99% Analysis Date = 10/20/16 Pct Recovery = 99% Analysis Date = 10/15/16 Pct Recovery = 99% Analysis Date = 10/15/16 Pct Recovery = 99% Analysis Date = 10/10/16 Pct Recovery = 98% Analysis Date = 10/10/16 Pct Recovery = 98% Analysis Date = 10/06/16 Pct Recovery = 98% Analysis Date = 10/06/16 Pct Recovery = 98% Analysis Date = 10/01/16 Pct Recovery = 98% Analysis Date = 10/01/16 Pct Recovery = 98% Analysis Date = 09/26/16 Pct Recovery = 98% Analysis Date = 09/26/16 Pct Recovery = 98% Analysis Date = 09/21/16 Pct Recovery = 98% Analysis Date = 09/21/16 Pct Recovery = 98% Analysis Date = 09/16/16 Pct Recovery = 98% Analysis Date = 09/16/16 Pct Recovery = 98% Analysis Date = 09/12/16 Pct Recovery = 98% Analysis Date = 09/12/16 Pct Recovery = 98% Analysis Date = 09/07/16 Pct Recovery = 98% Analysis Date = 09/07/16 Pct Recovery = 98% Analysis Date = 09/02/16 Pct Recovery = 98% Analysis Date = 09/02/16 Pct Recovery = 98% Analysis Date = 08/28/16 Pct Recovery = 98% Analysis Date = 08/28/16 Pct Recovery = 98% Analysis Date = 08/24/16 Pct Recovery = 98% Analysis Date = 08/24/16 Pct Recovery = 98% Analysis Date = 08/19/16 Pct Recovery = 98% Analysis Date = 08/19/16 Pct Recovery = 98% Analysis Date = 08/14/16 Pct Recovery = 98% Analysis Date = 08/14/16 Pct Recovery = 98% Analysis Date = 08/09/16 Pct Recovery = 98% Analysis Date = 08/09/16 Pct Recovery = 98% Analysis Date = 08/04/16 Pct Recovery = 97% Analysis Date = 08/04/16 Pct Recovery = 97% Analysis Date = 07/31/16 Pct Recovery = 97% Analysis Date = 07/31/16 Pct Recovery = 97% Analysis Date = 07/26/16 Pct Recovery = 97% Analysis Date = 07/26/16 Pct Recovery = 97% Analysis Date = 07/21/16 Pct Recovery = 97% Analysis Date = 07/21/16 Pct Recovery = 97% Analysis Date = 07/16/16 Pct Recovery = 97% Analysis Date = 07/16/16 Pct Recovery = 97% Analysis Date = 07/12/16 Pct Recovery = 97% Analysis Date = 07/12/16 Pct Recovery = 97% Analysis Date = 07/07/16 Pct Recovery = 97% Analysis Date = 07/07/16 Pct Recovery = 97% Analysis Date = 07/02/16 Pct Recovery = 97% Analysis Date = 07/02/16 Pct Recovery = 97% Analysis Date = 06/27/16 Pct Recovery = 97% Analysis Date = 06/27/16 Pct Recovery = 97% Analysis Date = 06/22/16 Pct Recovery = 97% Analysis Date = 06/22/16 Pct Recovery = 97% Analysis Date = 06/18/16 Pct Recovery = 97% Analysis Date = 06/18/16 Pct Recovery = 97% Analysis Date = 06/13/16 Pct Recovery = 97% Analysis Date = 06/13/16 Pct Recovery = 97% Analysis Date = 06/08/16 Pct Recovery = 97% Analysis Date = 06/08/16 Pct Recovery = 97% Analysis Date = 06/03/16 Pct Recovery = 97% Analysis Date = 06/03/16 Pct Recovery = 97% Analysis Date = 05/30/16 Pct Recovery = 96% Analysis Date = 05/30/16 Pct Recovery = 96% Analysis Date = 05/25/16 Pct Recovery = 96% Analysis Date = 05/25/16 Pct Recovery = 96% Analysis Date = 05/20/16 Pct Recovery = 96% Analysis Date = 05/20/16 Pct Recovery = 96% Analysis Date = 05/15/16 Pct Recovery = 96% Analysis Date = 05/15/16 Pct Recovery = 96% Analysis Date = 05/10/16 Pct Recovery = 96% Analysis Date = 05/10/16 Pct Recovery = 96% Analysis Date = 05/06/16 Pct Recovery = 96% Analysis Date = 05/06/16 Pct Recovery = 96% Analysis Date = 05/01/16 Pct Recovery = 96% Analysis Date = 05/01/16 Pct Recovery = 96% Analysis Date = 04/26/16 Pct Recovery = 96% Analysis Date = 04/26/16 Pct Recovery = 96% Analysis Date = 04/21/16 Pct Recovery = 96% Analysis Date = 04/21/16 Pct Recovery = 96% Analysis Date = 04/16/16 Pct Recovery = 96% Analysis Date = 04/16/16 Pct Recovery = 96% Analysis Date = 04/12/16 Pct Recovery = 96% Analysis Date = 04/12/16 Pct Recovery = 96% Analysis Date = 04/07/16 Pct Recovery = 96% Analysis Date = 04/07/16 Pct Recovery = 96% Analysis Date = 04/02/16 Pct Recovery = 96% Analysis Date = 04/02/16 Pct Recovery = 96% Analysis Date = 03/28/16 Pct Recovery = 96% Analysis Date = 03/28/16 Pct Recovery = 96% Analysis Date = 03/24/16 Pct Recovery = 95% Analysis Date = 03/24/16 Pct Recovery = 95% Analysis Date = 03/19/16 Pct Recovery = 95% Analysis Date = 03/19/16 Pct Recovery = 95% Analysis Date = 03/14/16 Pct Recovery = 95% Analysis Date = 03/14/16 Pct Recovery = 95% Analysis Date = 03/09/16 Pct Recovery = 95% Analysis Date = 03/09/16 Pct Recovery = 95% Analysis Date = 03/04/16 Pct Recovery = 95% Analysis Date = 03/04/16 Pct Recovery = 95% Analysis Date = 02/29/16 Pct Recovery = 95% Analysis Date = 02/29/16 Pct Recovery = 95% Analysis Date = 02/24/16 Pct Recovery = 95% Analysis Date = 02/24/16 Pct Recovery = 95% Analysis Date = 02/19/16 Pct Recovery = 95% Analysis Date = 02/19/16 Pct Recovery = 95% Analysis Date = 02/14/16 Pct Recovery = 95% Analysis Date = 02/14/16 Pct Recovery = 95% Analysis Date = 02/10/16 Pct Recovery = 95% Analysis Date = 02/10/16 Pct Recovery = 95% Analysis Date = 02/05/16 Pct Recovery = 95% Analysis Date = 02/05/16 Pct Recovery = 95% Analysis Date = 01/31/16 Pct Recovery = 95% Analysis Date = 01/31/16 Pct Recovery = 95% Analysis Date = 01/26/16 Pct Recovery = 95% Analysis Date = 01/26/16 Pct Recovery = 95% Analysis Date = 01/21/16 Pct Recovery = 94% Analysis Date = 01/21/16 Pct Recovery = 94% Analysis Date = 01/17/16 Pct Recovery = 94% Analysis Date = 01/17/16 Pct Recovery = 94% Analysis Date = 01/12/16 Pct Recovery = 94% Analysis Date = 01/12/16 Pct Recovery = 94% Analysis Date = 01/07/16 Pct Recovery = 94% Analysis Date = 01/07/16 Pct Recovery = 94% Analysis Date = 01/02/16 Pct Recovery = 94% Analysis Date = 01/02/16 Pct Recovery = 94% Analysis Date = 12/29/15 Pct Recovery = 94% Analysis Date = 12/29/15 Pct Recovery = 94% Analysis Date = 12/24/15 Pct Recovery = 94% Analysis Date = 12/24/15 Pct Recovery = 94% Analysis Date = 12/19/15 Pct Recovery = 94% Analysis Date = 12/19/15 Pct Recovery = 94% Analysis Date = 12/14/15 Pct Recovery = 94% Analysis Date = 12/14/15 Pct Recovery = 94% Analysis Date = 12/09/15 Pct Recovery = 94% Analysis Date = 12/09/15 Pct Recovery = 94% Analysis Date = 12/05/15 Pct Recovery = 94% Analysis Date = 12/05/15 Pct Recovery = 94% Analysis Date = 11/30/15 Pct Recovery = 94% Analysis Date = 11/30/15 Pct Recovery = 94% Analysis Date = 11/25/15 Pct Recovery = 94% Analysis Date = 11/25/15 Pct Recovery = 94% Analysis Date = 11/20/15 Pct Recovery = 93% Analysis Date = 11/20/15 Pct Recovery = 93% Analysis Date = 11/16/15 Pct Recovery = 93% Analysis Date = 11/16/15 Pct Recovery = 93% Analysis Date = 11/11/15 Pct Recovery = 93% Analysis Date = 11/11/15 Pct Recovery = 93% Analysis Date = 11/06/15 Pct Recovery = 93% Analysis Date = 11/06/15 Pct Recovery = 93% Analysis Date = 11/01/15 Pct Recovery = 93% Analysis Date = 11/01/15 Pct Recovery = 93% Analysis Date = 10/27/15 Pct Recovery = 93% Analysis Date = 10/27/15 Pct Recovery = 93% Analysis Date = 10/23/15 Pct Recovery = 93% Analysis Date = 10/23/15 Pct Recovery = 93% Analysis Date = 10/18/15 Pct Recovery = 93% Analysis Date = 10/18/15 Pct Recovery = 93% Analysis Date = 10/13/15 Pct Recovery = 93% Analysis Date = 10/13/15 Pct Recovery = 93% Analysis Date = 10/08/15 Pct Recovery = 93% Analysis Date = 10/08/15 Pct Recovery = 93% Analysis Date = 10/04/15 Pct Recovery = 93% Analysis Date = 10/04/15 Pct Recovery = 93% Analysis Date = 09/29/15 Pct Recovery = 93% Analysis Date = 09/29/15 Pct Recovery = 93% Analysis Date = 09/24/15 Pct Recovery = 93% Analysis Date = 09/24/15 Pct Recovery = 93% Analysis Date = 09/19/15 Pct Recovery = 93% Analysis Date = 09/19/15 Pct Recovery = 93% Analysis Date = 09/14/15 Pct Recovery = 93% Analysis Date = 09/14/15 Pct Recovery = 93% Analysis Date = 09/10/15 Pct Recovery = 93% Analysis Date = 09/10/15 Pct Recovery = 93% Analysis Date = 09/05/15 Pct Recovery = 93% Analysis Date = 09/05/15 Pct Recovery = 93% Analysis Date = 08/31/15 Pct Recovery = 93% Analysis Date = 08/31/15 Pct Recovery = 93% Analysis Date = 08/26/15 Pct Recovery = 93% Analysis Date = 08/26/15 Pct Recovery = 93% Analysis Date = 08/21/15 Pct Recovery = 93% Analysis Date = 08/21/15 Pct Recovery = 93% Analysis Date = 08/17/15 Pct Recovery = 93% Analysis Date = 08/17/15 Pct Recovery = 93% Analysis Date = 08/12/15 Pct Recovery = 93% Analysis Date = 08/12/15 Pct Recovery = 93% Analysis Date = 08/07/15 Pct Recovery = 93% Analysis Date = 08/07/15 Pct Recovery = 93% Analysis Date = 08/02/15 Pct Recovery = 93% Analysis Date = 08/02/15 Pct Recovery = 93% Analysis Date = 07/29/15 Pct Recovery = 93% Analysis Date = 07/29/15 Pct Recovery = 93% Analysis Date = 07/24/15 Pct Recovery = 93% Analysis Date = 07/24/15 Pct Recovery = 93% Analysis Date = 07/19/15 Pct Recovery = 93% Analysis Date = 07/19/15 Pct Recovery = 93% Analysis Date = 07/14/15 Pct Recovery = 93% Analysis Date = 07/14/15 Pct Recovery = 93% Analysis Date = 07/09/15 Pct Recovery = 93% Analysis Date = 07/09/15 Pct Recovery = 93% Analysis Date = 07/05/15 Pct Recovery = 93% Analysis Date = 07/05/15 Pct Recovery = 93% Analysis Date = 06/30/15 Pct Recovery = 93% Analysis Date = 06/30/15 Pct Recovery = 93% Analysis Date = 06/25/15 Pct Recovery = 93% Analysis Date = 06/25/15 Pct Recovery = 93% Analysis Date = 06/20/15 Pct Recovery = 93% Analysis Date = 06/20/15 Pct Recovery = 93% Analysis Date = 06/16/15 Pct Recovery = 94% Analysis Date = 06/16/15 Pct Recovery = 94% Analysis Date = 06/11/15 Pct Recovery = 94% Analysis Date = 06/11/15 Pct Recovery = 94% Analysis Date = 06/06/15 Pct Recovery = 94% Analysis Date = 06/06/15 Pct Recovery = 94% Analysis Date = 06/01/15 Pct Recovery = 94% Analysis Date = 06/01/15 Pct Recovery = 94% Analysis Date = 05/27/15 Pct Recovery = 94% Analysis Date = 05/27/15 Pct Recovery = 94% Analysis Date = 05/23/15 Pct Recovery = 94% Analysis Date = 05/23/15 Pct Recovery = 94% Analysis Date = 05/18/15 Pct Recovery = 94% Analysis Date = 05/18/15 Pct Recovery = 94% Analysis Date = 05/13/15 Pct Recovery = 94% Analysis Date = 05/13/15 Pct Recovery = 94% Analysis Date = 05/08/15 Pct Recovery = 94% Analysis Date = 05/08/15 Pct Recovery = 94% Analysis Date = 05/04/15 Pct Recovery = 94% Analysis Date = 05/04/15 Pct Recovery = 94% Analysis Date = 04/29/15 Pct Recovery = 94% Analysis Date = 04/29/15 Pct Recovery = 94% Analysis Date = 04/24/15 Pct Recovery = 94% Analysis Date = 04/24/15 Pct Recovery = 94% Analysis Date = 04/19/15 Pct Recovery = 94% Analysis Date = 04/19/15 Pct Recovery = 94% Analysis Date = 04/14/15 Pct Recovery = 94% Analysis Date = 04/14/15 Pct Recovery = 94% Analysis Date = 04/10/15 Pct Recovery = 94% Analysis Date = 04/10/15 Pct Recovery = 94% Analysis Date = 04/05/15 Pct Recovery = 94% Analysis Date = 04/05/15 Pct Recovery = 94% Analysis Date = 03/31/15 Pct Recovery = 95% Analysis Date = 03/31/15 Pct Recovery = 95% Analysis Date = 03/26/15 Pct Recovery = 95% Analysis Date = 03/26/15 Pct Recovery = 95% Analysis Date = 03/22/15 Pct Recovery = 95% Analysis Date = 03/22/15 Pct Recovery = 95% Analysis Date = 03/17/15 Pct Recovery = 95% Analysis Date = 03/17/15 Pct Recovery = 95% Analysis Date = 03/12/15 Pct Recovery = 95% Analysis Date = 03/12/15 Pct Recovery = 95% Analysis Date = 03/07/15 Pct Recovery = 96% Analysis Date = 03/07/15 Pct Recovery = 96% Analysis Date = 03/02/15 Pct Recovery = 96% Analysis Date = 03/02/15 Pct Recovery = 96% Analysis Date = 02/26/15 Pct Recovery = 96% Analysis Date = 02/26/15 Pct Recovery = 96% Analysis Date = 02/21/15 Pct Recovery = 96% Analysis Date = 02/21/15 Pct Recovery = 96% Analysis Date = 02/16/15 Pct Recovery = 96% Analysis Date = 02/16/15 Pct Recovery = 96% Analysis Date = 02/11/15 Pct Recovery = 97% Analysis Date = 02/11/15 Pct Recovery = 97% Analysis Date = 02/07/15 Pct Recovery = 97% Analysis Date = 02/07/15 Pct Recovery = 97% Analysis Date = 02/02/15 Pct Recovery = 97% Analysis Date = 02/02/15 Pct Recovery = 97% Analysis Date = 01/28/15 Pct Recovery = 97% Analysis Date = 01/28/15 Pct Recovery = 97% Analysis Date = 01/23/15 Pct Recovery = 97% Analysis Date = 01/23/15 Pct Recovery = 97% Analysis Date = 01/18/15 Pct Recovery = 98% Analysis Date = 01/18/15 Pct Recovery = 98% Analysis Date = 01/14/15 Pct Recovery = 98% Analysis Date = 01/14/15 Pct Recovery = 98% Analysis Date = 01/09/15 Pct Recovery = 98% Analysis Date = 01/09/15 Pct Recovery = 98% Analysis Date = 01/04/15 Pct Recovery = 98% Analysis Date = 01/04/15 Pct Recovery = 98% Analysis Date = 12/30/14 Pct Recovery = 98% Analysis Date = 12/30/14 Pct Recovery = 98% Analysis Date = 12/25/14 Pct Recovery = 99% Analysis Date = 12/25/14 Pct Recovery = 99% Analysis Date = 12/21/14 Pct Recovery = 99% Analysis Date = 12/21/14 Pct Recovery = 99% Analysis Date = 12/16/14 Pct Recovery = 99% Analysis Date = 12/16/14 Pct Recovery = 99% Analysis Date = 12/11/14 Pct Recovery = 99% Analysis Date = 12/11/14 Pct Recovery = 99% Analysis Date = 12/06/14 Pct Recovery = 99% Analysis Date = 12/06/14 Pct Recovery = 99% Analysis Date = 12/02/14 Pct Recovery = 100% Analysis Date = 12/02/14 Pct Recovery = 100% Analysis Date = 11/27/14 Pct Recovery = 100% Analysis Date = 11/27/14 Pct Recovery = 100% Analysis Date = 11/22/14 Pct Recovery = 100% Analysis Date = 11/22/14 Pct Recovery = 100% Analysis Date = 11/17/14 Pct Recovery = 100% Analysis Date = 11/17/14 Pct Recovery = 100% Analysis Date = 11/12/14 Pct Recovery = 100% Analysis Date = 11/12/14 Pct Recovery = 100% Analysis Date = 11/08/14 Pct Recovery = 100% Analysis Date = 11/08/14 Pct Recovery = 100% Analysis Date = 11/03/14 Pct Recovery = 101% Analysis Date = 11/03/14 Pct Recovery = 101% Analysis Date = 10/29/14 Pct Recovery = 101% Analysis Date = 10/29/14 Pct Recovery = 101% Analysis Date = 10/24/14 Pct Recovery = 101% Analysis Date = 10/24/14 Pct Recovery = 101% Analysis Date = 10/20/14 Pct Recovery = 101% Analysis Date = 10/20/14 Pct Recovery = 101% Analysis Date = 10/15/14 Pct Recovery = 101% Analysis Date = 10/15/14 Pct Recovery = 101% Analysis Date = 10/10/14 Pct Recovery = 101% Analysis Date = 10/10/14 Pct Recovery = 101% Analysis Date = 10/05/14 Pct Recovery = 102% Analysis Date = 10/05/14 Pct Recovery = 102% Analysis Date = 09/30/14 Pct Recovery = 102% Analysis Date = 09/30/14 Pct Recovery = 102% Analysis Date = 09/26/14 Pct Recovery = 102% Analysis Date = 09/26/14 Pct Recovery = 102% Analysis Date = 09/21/14 Pct Recovery = 102% Analysis Date = 09/21/14 Pct Recovery = 102% Analysis Date = 09/16/14 Pct Recovery = 102% Analysis Date = 09/16/14 Pct Recovery = 102% Analysis Date = 09/11/14 Pct Recovery = 102% Analysis Date = 09/11/14 Pct Recovery = 102% Analysis Date = 09/07/14 Pct Recovery = 103% Analysis Date = 09/07/14 Pct Recovery = 103% Analysis Date = 09/02/14 Pct Recovery = 103% Analysis Date = 09/02/14 Pct Recovery = 103% Analysis Date = 08/28/14 Pct Recovery = 103% Analysis Date = 08/28/14 Pct Recovery = 103% Analysis Date = 08/23/14 Pct Recovery = 103% Analysis Date = 08/23/14 Pct Recovery = 103% Analysis Date = 08/18/14 Pct Recovery = 103% Analysis Date = 08/18/14 Pct Recovery = 103% Analysis Date = 08/14/14 Pct Recovery = 103% Analysis Date = 08/14/14 Pct Recovery = 103% Analysis Date = 08/09/14 Pct Recovery = 104% Analysis Date = 08/09/14 Pct Recovery = 104% Analysis Date = 08/04/14 Pct Recovery = 104% Analysis Date = 08/04/14 Pct Recovery = 104% Analysis Date = 07/30/14 Pct Recovery = 104% Analysis Date = 07/30/14 Pct Recovery = 104% Analysis Date = 07/26/14 Pct Recovery = 104% Analysis Date = 07/26/14 Pct Recovery = 104% Analysis Date = 07/21/14 Pct Recovery = 104% Analysis Date = 07/21/14 Pct Recovery = 104% Analysis Date = 07/16/14 Pct Recovery = 104% Analysis Date = 07/16/14 Pct Recovery = 104% Analysis Date = 07/11/14 Pct Recovery = 105% Analysis Date = 07/11/14 Pct Recovery = 105% Analysis Date = 07/06/14 Pct Recovery = 105% Analysis Date = 07/06/14 Pct Recovery = 105% Analysis Date = 07/02/14 Pct Recovery = 105% Analysis Date = 07/02/14 Pct Recovery = 105% Analysis Date = 06/27/14 Pct Recovery = 105% Analysis Date = 06/27/14 Pct Recovery = 105% Analysis Date = 06/22/14 Pct Recovery = 105% Analysis Date = 06/22/14 Pct Recovery = 105% Analysis Date = 06/17/14 Pct Recovery = 105% Analysis Date = 06/17/14 Pct Recovery = 105% Analysis Date = 06/13/14 Pct Recovery = 106% Analysis Date = 06/13/14 Pct Recovery = 106% Analysis Date = 06/08/14 Pct Recovery = 106% Analysis Date = 06/08/14 Pct Recovery = 106% Analysis Date = 06/03/14 Pct Recovery = 106% Analysis Date = 06/03/14 Pct Recovery = 106% Analysis Date = 05/29/14 Pct Recovery = 106% Analysis Date = 05/29/14 Pct Recovery = 106% Analysis Date = 05/24/14 Pct Recovery = 106% Analysis Date = 05/24/14 Pct Recovery = 106% Analysis Date = 05/20/14 Pct Recovery = 106% Analysis Date = 05/20/14 Pct Recovery = 106% Analysis Date = 05/15/14 Pct Recovery = 106% Analysis Date = 05/15/14 Pct Recovery = 106% Analysis Date = 05/10/14 Pct Recovery = 107% Analysis Date = 05/10/14 Pct Recovery = 107% Analysis Date = 05/05/14 Pct Recovery = 107% Analysis Date = 05/05/14 Pct Recovery = 107% Analysis Date = 05/01/14 Pct Recovery = 107% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
DIBROMOMETHANE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 43 98% 8% 97% 9%
Total 43 98% 8% 97% 9%

Sample Statistics
DIBROMOMETHANE

Characteristic N % % Basis
Plotted 43 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 43 .  
False Negatives 0 0% 0 out of 43
Not Spiked 23 .  
False Positives 0 0% 0 out of 23

BQS OBSP Determination:
DICHLORODIFLUOROMETHANE
METHOD: 4440 , TESTIDCODE: 34668GCM66
Open Data Set

Analysis Date = 12/16/16 SpikeMix = NSI 041816AVOC: 40 µl & ChemService 5082900: 40 µl Pct Recovery = 52% Analysis Date = 12/12/16 SpikeMix = Accu 216041125: 40 µl & Crescent 03FF058: 40 µl Pct Recovery = 63% Analysis Date = 08/04/16 SpikeMix = Crescent 03FF058: 40 µl & Supelco LC20141V: 40 µl Pct Recovery = 73% Analysis Date = 07/14/16 SpikeMix = Accu 216041125: 40 µl & NSI 041816AVOC: 40 µl Pct Recovery = 65% Analysis Date = 11/21/16 SpikeMix = Crescent 03FF058: 25 µl & Supelco LC20141V: 25 µl Pct Recovery = 50% Analysis Date = 08/26/16 SpikeMix = NSI 041816AVOC: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 54% Analysis Date = 06/30/16 SpikeMix = Crescent 03FF058: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 64% Analysis Date = 06/21/16 SpikeMix = Phenova B20160319: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 62% Analysis Date = 05/24/16 SpikeMix = Accu 216041125: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 62% Analysis Date = 11/22/14 SpikeMix = NSI 032614: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 141% Analysis Date = 06/10/14 SpikeMix = Crescent 03DD004: 20 µl & NSI 032614: 20 µl Pct Recovery = 145% Analysis Date = 06/10/14 SpikeMix = NSI 032614: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 152% Analysis Date = 05/01/14 SpikeMix = Accu 214031115: 20 µl & NSI 032614: 20 µl Pct Recovery = 138% Analysis Date = 04/09/15 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 96% Analysis Date = 03/06/15 SpikeMix = ERA 0227-14-06.1A: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 122% Analysis Date = 11/14/14 SpikeMix = Crescent 03DD004: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 111% Analysis Date = 08/16/14 SpikeMix = ERA 0227-14-06.1A: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 143% Analysis Date = 07/01/14 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 160% Analysis Date = 08/15/15 SpikeMix = Supelco LC13545: 25 µl & Crescent 04EE008: 25 µl Pct Recovery = 73% Analysis Date = 07/13/15 SpikeMix = Crescent 04EE008: 25 µl & NSI 050515AVOC: 25 µl Pct Recovery = 63% Analysis Date = 09/29/15 SpikeMix = Accu 215041380: 25 µl & ERA 0406-15-03: 25 µl Pct Recovery = 60% Analysis Date = 10/13/16 SpikeMix = Accu 216041125: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 63% Analysis Date = 10/13/16 SpikeMix = NSI 041816AVOC: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 55% Analysis Date = 09/28/16 SpikeMix = Crescent 03FF058: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 69% Analysis Date = 09/08/16 SpikeMix = Phenova B20160319: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 69% Analysis Date = 08/20/16 SpikeMix = Accu 216041125: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 66% Analysis Date = 07/29/16 SpikeMix = Phenova B20160319: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 61% Analysis Date = 06/10/16 SpikeMix = NSI 041816AVOC: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 63% Analysis Date = 12/18/15 SpikeMix = Supelco LC13545: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 68% Analysis Date = 10/17/15 SpikeMix = Crescent 04EE008: 15 µl & NSI 050515AVOC: 15 µl Pct Recovery = 60% Analysis Date = 05/09/15 SpikeMix = Spex Organics EN150428007: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 76% Analysis Date = 04/02/16 SpikeMix = Supelco LC13545: 15 µl & Accu 215041380: 15 µl Pct Recovery = 78% Analysis Date = 03/04/16 SpikeMix = Accu 215041380: 15 µl & ERA 0406-15-03: 15 µl Pct Recovery = 66% Analysis Date = 06/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Accu 215041380: 15 µl Pct Recovery = 79% Analysis Date = 09/09/14 SpikeMix = Accu 214031115: 10 µl & NSI 032614: 10 µl Pct Recovery = 175% Analysis Date = 09/09/14 SpikeMix = NSI 032614: 10 µl & Spex Organics C1140417015: 10 µl Pct Recovery = 167% Analysis Date = 07/29/14 SpikeMix = Crescent 03DD004: 10 µl & NSI 032614: 10 µl Pct Recovery = 148% Analysis Date = 05/30/14 SpikeMix = NSI 032614: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 136% Analysis Date = 01/13/15 SpikeMix = Accu 214031115: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 120% Analysis Date = 10/21/14 SpikeMix = ERA 0227-14-06.1A: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 117% Analysis Date = 10/04/14 SpikeMix = Crescent 03DD004: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 109% Analysis Date = 07/11/14 SpikeMix = Spex Organics C1140417015: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 107% Analysis Date = 05/13/16 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 51% Analysis Date = 01/27/16 SpikeMix = Crescent 04EE008: 10 µl & NSI 050515AVOC: 10 µl Pct Recovery = 68% Analysis Date = 07/31/15 SpikeMix = Crescent 04EE008: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 63% Analysis Date = 05/09/15 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 75% Analysis Date = 02/18/16 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 70% Analysis Date = 11/20/15 SpikeMix = Accu 215041380: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 79% Analysis Date = 11/12/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 76% Analysis Date = 05/21/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 80% Analysis Date = 12/15/16 Pct Recovery = 58% Analysis Date = 12/11/16 Pct Recovery = 58% Analysis Date = 12/11/16 Pct Recovery = 58% Analysis Date = 12/06/16 Pct Recovery = 59% Analysis Date = 12/06/16 Pct Recovery = 59% Analysis Date = 12/01/16 Pct Recovery = 59% Analysis Date = 12/01/16 Pct Recovery = 59% Analysis Date = 11/26/16 Pct Recovery = 59% Analysis Date = 11/26/16 Pct Recovery = 59% Analysis Date = 11/21/16 Pct Recovery = 59% Analysis Date = 11/21/16 Pct Recovery = 59% Analysis Date = 11/17/16 Pct Recovery = 59% Analysis Date = 11/17/16 Pct Recovery = 59% Analysis Date = 11/12/16 Pct Recovery = 59% Analysis Date = 11/12/16 Pct Recovery = 59% Analysis Date = 11/07/16 Pct Recovery = 60% Analysis Date = 11/07/16 Pct Recovery = 60% Analysis Date = 11/02/16 Pct Recovery = 60% Analysis Date = 11/02/16 Pct Recovery = 60% Analysis Date = 10/28/16 Pct Recovery = 60% Analysis Date = 10/28/16 Pct Recovery = 60% Analysis Date = 10/24/16 Pct Recovery = 60% Analysis Date = 10/24/16 Pct Recovery = 60% Analysis Date = 10/19/16 Pct Recovery = 60% Analysis Date = 10/19/16 Pct Recovery = 60% Analysis Date = 10/14/16 Pct Recovery = 60% Analysis Date = 10/14/16 Pct Recovery = 60% Analysis Date = 10/09/16 Pct Recovery = 60% Analysis Date = 10/09/16 Pct Recovery = 60% Analysis Date = 10/04/16 Pct Recovery = 61% Analysis Date = 10/04/16 Pct Recovery = 61% Analysis Date = 09/30/16 Pct Recovery = 61% Analysis Date = 09/30/16 Pct Recovery = 61% Analysis Date = 09/25/16 Pct Recovery = 61% Analysis Date = 09/25/16 Pct Recovery = 61% Analysis Date = 09/20/16 Pct Recovery = 61% Analysis Date = 09/20/16 Pct Recovery = 61% Analysis Date = 09/15/16 Pct Recovery = 61% Analysis Date = 09/15/16 Pct Recovery = 61% Analysis Date = 09/10/16 Pct Recovery = 61% Analysis Date = 09/10/16 Pct Recovery = 61% Analysis Date = 09/06/16 Pct Recovery = 62% Analysis Date = 09/06/16 Pct Recovery = 62% Analysis Date = 09/01/16 Pct Recovery = 62% Analysis Date = 09/01/16 Pct Recovery = 62% Analysis Date = 08/27/16 Pct Recovery = 62% Analysis Date = 08/27/16 Pct Recovery = 62% Analysis Date = 08/22/16 Pct Recovery = 62% Analysis Date = 08/22/16 Pct Recovery = 62% Analysis Date = 08/17/16 Pct Recovery = 62% Analysis Date = 08/17/16 Pct Recovery = 62% Analysis Date = 08/13/16 Pct Recovery = 62% Analysis Date = 08/13/16 Pct Recovery = 62% Analysis Date = 08/08/16 Pct Recovery = 62% Analysis Date = 08/08/16 Pct Recovery = 62% Analysis Date = 08/03/16 Pct Recovery = 63% Analysis Date = 08/03/16 Pct Recovery = 63% Analysis Date = 07/29/16 Pct Recovery = 63% Analysis Date = 07/29/16 Pct Recovery = 63% Analysis Date = 07/24/16 Pct Recovery = 63% Analysis Date = 07/24/16 Pct Recovery = 63% Analysis Date = 07/20/16 Pct Recovery = 63% Analysis Date = 07/20/16 Pct Recovery = 63% Analysis Date = 07/15/16 Pct Recovery = 63% Analysis Date = 07/15/16 Pct Recovery = 63% Analysis Date = 07/10/16 Pct Recovery = 63% Analysis Date = 07/10/16 Pct Recovery = 63% Analysis Date = 07/05/16 Pct Recovery = 64% Analysis Date = 07/05/16 Pct Recovery = 64% Analysis Date = 06/30/16 Pct Recovery = 64% Analysis Date = 06/30/16 Pct Recovery = 64% Analysis Date = 06/26/16 Pct Recovery = 64% Analysis Date = 06/26/16 Pct Recovery = 64% Analysis Date = 06/21/16 Pct Recovery = 64% Analysis Date = 06/21/16 Pct Recovery = 64% Analysis Date = 06/16/16 Pct Recovery = 64% Analysis Date = 06/16/16 Pct Recovery = 64% Analysis Date = 06/11/16 Pct Recovery = 64% Analysis Date = 06/11/16 Pct Recovery = 64% Analysis Date = 06/06/16 Pct Recovery = 64% Analysis Date = 06/06/16 Pct Recovery = 64% Analysis Date = 06/02/16 Pct Recovery = 64% Analysis Date = 06/02/16 Pct Recovery = 64% Analysis Date = 05/28/16 Pct Recovery = 65% Analysis Date = 05/28/16 Pct Recovery = 65% Analysis Date = 05/23/16 Pct Recovery = 65% Analysis Date = 05/23/16 Pct Recovery = 65% Analysis Date = 05/18/16 Pct Recovery = 65% Analysis Date = 05/18/16 Pct Recovery = 65% Analysis Date = 05/13/16 Pct Recovery = 65% Analysis Date = 05/13/16 Pct Recovery = 65% Analysis Date = 05/09/16 Pct Recovery = 65% Analysis Date = 05/09/16 Pct Recovery = 65% Analysis Date = 05/04/16 Pct Recovery = 65% Analysis Date = 05/04/16 Pct Recovery = 65% Analysis Date = 04/29/16 Pct Recovery = 65% Analysis Date = 04/29/16 Pct Recovery = 65% Analysis Date = 04/24/16 Pct Recovery = 65% Analysis Date = 04/24/16 Pct Recovery = 65% Analysis Date = 04/19/16 Pct Recovery = 65% Analysis Date = 04/19/16 Pct Recovery = 65% Analysis Date = 04/15/16 Pct Recovery = 66% Analysis Date = 04/15/16 Pct Recovery = 66% Analysis Date = 04/10/16 Pct Recovery = 66% Analysis Date = 04/10/16 Pct Recovery = 66% Analysis Date = 04/05/16 Pct Recovery = 66% Analysis Date = 04/05/16 Pct Recovery = 66% Analysis Date = 03/31/16 Pct Recovery = 66% Analysis Date = 03/31/16 Pct Recovery = 66% Analysis Date = 03/26/16 Pct Recovery = 66% Analysis Date = 03/26/16 Pct Recovery = 66% Analysis Date = 03/22/16 Pct Recovery = 66% Analysis Date = 03/22/16 Pct Recovery = 66% Analysis Date = 03/17/16 Pct Recovery = 66% Analysis Date = 03/17/16 Pct Recovery = 66% Analysis Date = 03/12/16 Pct Recovery = 66% Analysis Date = 03/12/16 Pct Recovery = 66% Analysis Date = 03/07/16 Pct Recovery = 67% Analysis Date = 03/07/16 Pct Recovery = 67% Analysis Date = 03/02/16 Pct Recovery = 67% Analysis Date = 03/02/16 Pct Recovery = 67% Analysis Date = 02/27/16 Pct Recovery = 67% Analysis Date = 02/27/16 Pct Recovery = 67% Analysis Date = 02/22/16 Pct Recovery = 67% Analysis Date = 02/22/16 Pct Recovery = 67% Analysis Date = 02/17/16 Pct Recovery = 67% Analysis Date = 02/17/16 Pct Recovery = 67% Analysis Date = 02/12/16 Pct Recovery = 67% Analysis Date = 02/12/16 Pct Recovery = 67% Analysis Date = 02/07/16 Pct Recovery = 67% Analysis Date = 02/07/16 Pct Recovery = 67% Analysis Date = 02/03/16 Pct Recovery = 67% Analysis Date = 02/03/16 Pct Recovery = 67% Analysis Date = 01/29/16 Pct Recovery = 67% Analysis Date = 01/29/16 Pct Recovery = 67% Analysis Date = 01/24/16 Pct Recovery = 67% Analysis Date = 01/24/16 Pct Recovery = 67% Analysis Date = 01/19/16 Pct Recovery = 67% Analysis Date = 01/19/16 Pct Recovery = 67% Analysis Date = 01/14/16 Pct Recovery = 68% Analysis Date = 01/14/16 Pct Recovery = 68% Analysis Date = 01/10/16 Pct Recovery = 68% Analysis Date = 01/10/16 Pct Recovery = 68% Analysis Date = 01/05/16 Pct Recovery = 68% Analysis Date = 01/05/16 Pct Recovery = 68% Analysis Date = 12/31/15 Pct Recovery = 68% Analysis Date = 12/31/15 Pct Recovery = 68% Analysis Date = 12/26/15 Pct Recovery = 68% Analysis Date = 12/26/15 Pct Recovery = 68% Analysis Date = 12/21/15 Pct Recovery = 68% Analysis Date = 12/21/15 Pct Recovery = 68% Analysis Date = 12/17/15 Pct Recovery = 68% Analysis Date = 12/17/15 Pct Recovery = 68% Analysis Date = 12/12/15 Pct Recovery = 68% Analysis Date = 12/12/15 Pct Recovery = 68% Analysis Date = 12/07/15 Pct Recovery = 69% Analysis Date = 12/07/15 Pct Recovery = 69% Analysis Date = 12/02/15 Pct Recovery = 69% Analysis Date = 12/02/15 Pct Recovery = 69% Analysis Date = 11/27/15 Pct Recovery = 69% Analysis Date = 11/27/15 Pct Recovery = 69% Analysis Date = 11/23/15 Pct Recovery = 69% Analysis Date = 11/23/15 Pct Recovery = 69% Analysis Date = 11/18/15 Pct Recovery = 70% Analysis Date = 11/18/15 Pct Recovery = 70% Analysis Date = 11/13/15 Pct Recovery = 70% Analysis Date = 11/13/15 Pct Recovery = 70% Analysis Date = 11/08/15 Pct Recovery = 70% Analysis Date = 11/08/15 Pct Recovery = 70% Analysis Date = 11/03/15 Pct Recovery = 70% Analysis Date = 11/03/15 Pct Recovery = 70% Analysis Date = 10/30/15 Pct Recovery = 71% Analysis Date = 10/30/15 Pct Recovery = 71% Analysis Date = 10/25/15 Pct Recovery = 71% Analysis Date = 10/25/15 Pct Recovery = 71% Analysis Date = 10/20/15 Pct Recovery = 71% Analysis Date = 10/20/15 Pct Recovery = 71% Analysis Date = 10/15/15 Pct Recovery = 72% Analysis Date = 10/15/15 Pct Recovery = 72% Analysis Date = 10/10/15 Pct Recovery = 72% Analysis Date = 10/10/15 Pct Recovery = 72% Analysis Date = 10/06/15 Pct Recovery = 72% Analysis Date = 10/06/15 Pct Recovery = 72% Analysis Date = 10/01/15 Pct Recovery = 72% Analysis Date = 10/01/15 Pct Recovery = 72% Analysis Date = 09/26/15 Pct Recovery = 73% Analysis Date = 09/26/15 Pct Recovery = 73% Analysis Date = 09/21/15 Pct Recovery = 73% Analysis Date = 09/21/15 Pct Recovery = 73% Analysis Date = 09/16/15 Pct Recovery = 74% Analysis Date = 09/16/15 Pct Recovery = 74% Analysis Date = 09/12/15 Pct Recovery = 75% Analysis Date = 09/12/15 Pct Recovery = 75% Analysis Date = 09/07/15 Pct Recovery = 75% Analysis Date = 09/07/15 Pct Recovery = 75% Analysis Date = 09/02/15 Pct Recovery = 76% Analysis Date = 09/02/15 Pct Recovery = 76% Analysis Date = 08/28/15 Pct Recovery = 76% Analysis Date = 08/28/15 Pct Recovery = 76% Analysis Date = 08/23/15 Pct Recovery = 77% Analysis Date = 08/23/15 Pct Recovery = 77% Analysis Date = 08/19/15 Pct Recovery = 78% Analysis Date = 08/19/15 Pct Recovery = 78% Analysis Date = 08/14/15 Pct Recovery = 78% Analysis Date = 08/14/15 Pct Recovery = 78% Analysis Date = 08/09/15 Pct Recovery = 79% Analysis Date = 08/09/15 Pct Recovery = 79% Analysis Date = 08/04/15 Pct Recovery = 79% Analysis Date = 08/04/15 Pct Recovery = 79% Analysis Date = 07/30/15 Pct Recovery = 80% Analysis Date = 07/30/15 Pct Recovery = 80% Analysis Date = 07/26/15 Pct Recovery = 81% Analysis Date = 07/26/15 Pct Recovery = 81% Analysis Date = 07/21/15 Pct Recovery = 81% Analysis Date = 07/21/15 Pct Recovery = 81% Analysis Date = 07/16/15 Pct Recovery = 82% Analysis Date = 07/16/15 Pct Recovery = 82% Analysis Date = 07/11/15 Pct Recovery = 82% Analysis Date = 07/11/15 Pct Recovery = 82% Analysis Date = 07/06/15 Pct Recovery = 83% Analysis Date = 07/06/15 Pct Recovery = 83% Analysis Date = 07/02/15 Pct Recovery = 84% Analysis Date = 07/02/15 Pct Recovery = 84% Analysis Date = 06/27/15 Pct Recovery = 84% Analysis Date = 06/27/15 Pct Recovery = 84% Analysis Date = 06/22/15 Pct Recovery = 85% Analysis Date = 06/22/15 Pct Recovery = 85% Analysis Date = 06/17/15 Pct Recovery = 85% Analysis Date = 06/17/15 Pct Recovery = 85% Analysis Date = 06/12/15 Pct Recovery = 86% Analysis Date = 06/12/15 Pct Recovery = 86% Analysis Date = 06/08/15 Pct Recovery = 87% Analysis Date = 06/08/15 Pct Recovery = 87% Analysis Date = 06/03/15 Pct Recovery = 87% Analysis Date = 06/03/15 Pct Recovery = 87% Analysis Date = 05/29/15 Pct Recovery = 88% Analysis Date = 05/29/15 Pct Recovery = 88% Analysis Date = 05/24/15 Pct Recovery = 88% Analysis Date = 05/24/15 Pct Recovery = 88% Analysis Date = 05/19/15 Pct Recovery = 89% Analysis Date = 05/19/15 Pct Recovery = 89% Analysis Date = 05/15/15 Pct Recovery = 89% Analysis Date = 05/15/15 Pct Recovery = 89% Analysis Date = 05/10/15 Pct Recovery = 90% Analysis Date = 05/10/15 Pct Recovery = 90% Analysis Date = 05/05/15 Pct Recovery = 91% Analysis Date = 05/05/15 Pct Recovery = 91% Analysis Date = 04/30/15 Pct Recovery = 92% Analysis Date = 04/30/15 Pct Recovery = 92% Analysis Date = 04/25/15 Pct Recovery = 93% Analysis Date = 04/25/15 Pct Recovery = 93% Analysis Date = 04/21/15 Pct Recovery = 93% Analysis Date = 04/21/15 Pct Recovery = 93% Analysis Date = 04/16/15 Pct Recovery = 94% Analysis Date = 04/16/15 Pct Recovery = 94% Analysis Date = 04/11/15 Pct Recovery = 95% Analysis Date = 04/11/15 Pct Recovery = 95% Analysis Date = 04/06/15 Pct Recovery = 96% Analysis Date = 04/06/15 Pct Recovery = 96% Analysis Date = 04/01/15 Pct Recovery = 97% Analysis Date = 04/01/15 Pct Recovery = 97% Analysis Date = 03/28/15 Pct Recovery = 98% Analysis Date = 03/28/15 Pct Recovery = 98% Analysis Date = 03/23/15 Pct Recovery = 99% Analysis Date = 03/23/15 Pct Recovery = 99% Analysis Date = 03/18/15 Pct Recovery = 99% Analysis Date = 03/18/15 Pct Recovery = 99% Analysis Date = 03/13/15 Pct Recovery = 100% Analysis Date = 03/13/15 Pct Recovery = 100% Analysis Date = 03/08/15 Pct Recovery = 101% Analysis Date = 03/08/15 Pct Recovery = 101% Analysis Date = 03/04/15 Pct Recovery = 102% Analysis Date = 03/04/15 Pct Recovery = 102% Analysis Date = 02/27/15 Pct Recovery = 103% Analysis Date = 02/27/15 Pct Recovery = 103% Analysis Date = 02/22/15 Pct Recovery = 104% Analysis Date = 02/22/15 Pct Recovery = 104% Analysis Date = 02/17/15 Pct Recovery = 104% Analysis Date = 02/17/15 Pct Recovery = 104% Analysis Date = 02/12/15 Pct Recovery = 105% Analysis Date = 02/12/15 Pct Recovery = 105% Analysis Date = 02/08/15 Pct Recovery = 106% Analysis Date = 02/08/15 Pct Recovery = 106% Analysis Date = 02/03/15 Pct Recovery = 107% Analysis Date = 02/03/15 Pct Recovery = 107% Analysis Date = 01/29/15 Pct Recovery = 108% Analysis Date = 01/29/15 Pct Recovery = 108% Analysis Date = 01/24/15 Pct Recovery = 109% Analysis Date = 01/24/15 Pct Recovery = 109% Analysis Date = 01/19/15 Pct Recovery = 110% Analysis Date = 01/19/15 Pct Recovery = 110% Analysis Date = 01/15/15 Pct Recovery = 110% Analysis Date = 01/15/15 Pct Recovery = 110% Analysis Date = 01/10/15 Pct Recovery = 111% Analysis Date = 01/10/15 Pct Recovery = 111% Analysis Date = 01/05/15 Pct Recovery = 112% Analysis Date = 01/05/15 Pct Recovery = 112% Analysis Date = 12/31/14 Pct Recovery = 113% Analysis Date = 12/31/14 Pct Recovery = 113% Analysis Date = 12/26/14 Pct Recovery = 114% Analysis Date = 12/26/14 Pct Recovery = 114% Analysis Date = 12/22/14 Pct Recovery = 115% Analysis Date = 12/22/14 Pct Recovery = 115% Analysis Date = 12/17/14 Pct Recovery = 116% Analysis Date = 12/17/14 Pct Recovery = 116% Analysis Date = 12/12/14 Pct Recovery = 116% Analysis Date = 12/12/14 Pct Recovery = 116% Analysis Date = 12/07/14 Pct Recovery = 117% Analysis Date = 12/07/14 Pct Recovery = 117% Analysis Date = 12/02/14 Pct Recovery = 118% Analysis Date = 12/02/14 Pct Recovery = 118% Analysis Date = 11/28/14 Pct Recovery = 119% Analysis Date = 11/28/14 Pct Recovery = 119% Analysis Date = 11/23/14 Pct Recovery = 120% Analysis Date = 11/23/14 Pct Recovery = 120% Analysis Date = 11/18/14 Pct Recovery = 121% Analysis Date = 11/18/14 Pct Recovery = 121% Analysis Date = 11/13/14 Pct Recovery = 122% Analysis Date = 11/13/14 Pct Recovery = 122% Analysis Date = 11/08/14 Pct Recovery = 122% Analysis Date = 11/08/14 Pct Recovery = 122% Analysis Date = 11/04/14 Pct Recovery = 123% Analysis Date = 11/04/14 Pct Recovery = 123% Analysis Date = 10/30/14 Pct Recovery = 124% Analysis Date = 10/30/14 Pct Recovery = 124% Analysis Date = 10/25/14 Pct Recovery = 125% Analysis Date = 10/25/14 Pct Recovery = 125% Analysis Date = 10/20/14 Pct Recovery = 126% Analysis Date = 10/20/14 Pct Recovery = 126% Analysis Date = 10/15/14 Pct Recovery = 127% Analysis Date = 10/15/14 Pct Recovery = 127% Analysis Date = 10/11/14 Pct Recovery = 128% Analysis Date = 10/11/14 Pct Recovery = 128% Analysis Date = 10/06/14 Pct Recovery = 128% Analysis Date = 10/06/14 Pct Recovery = 128% Analysis Date = 10/01/14 Pct Recovery = 129% Analysis Date = 10/01/14 Pct Recovery = 129% Analysis Date = 09/26/14 Pct Recovery = 130% Analysis Date = 09/26/14 Pct Recovery = 130% Analysis Date = 09/21/14 Pct Recovery = 131% Analysis Date = 09/21/14 Pct Recovery = 131% Analysis Date = 09/17/14 Pct Recovery = 132% Analysis Date = 09/17/14 Pct Recovery = 132% Analysis Date = 09/12/14 Pct Recovery = 133% Analysis Date = 09/12/14 Pct Recovery = 133% Analysis Date = 09/07/14 Pct Recovery = 134% Analysis Date = 09/07/14 Pct Recovery = 134% Analysis Date = 09/02/14 Pct Recovery = 134% Analysis Date = 09/02/14 Pct Recovery = 134% Analysis Date = 08/28/14 Pct Recovery = 135% Analysis Date = 08/28/14 Pct Recovery = 135% Analysis Date = 08/24/14 Pct Recovery = 136% Analysis Date = 08/24/14 Pct Recovery = 136% Analysis Date = 08/19/14 Pct Recovery = 137% Analysis Date = 08/19/14 Pct Recovery = 137% Analysis Date = 08/14/14 Pct Recovery = 138% Analysis Date = 08/14/14 Pct Recovery = 138% Analysis Date = 08/09/14 Pct Recovery = 139% Analysis Date = 08/09/14 Pct Recovery = 139% Analysis Date = 08/04/14 Pct Recovery = 140% Analysis Date = 08/04/14 Pct Recovery = 140% Analysis Date = 07/31/14 Pct Recovery = 140% Analysis Date = 07/31/14 Pct Recovery = 140% Analysis Date = 07/26/14 Pct Recovery = 141% Analysis Date = 07/26/14 Pct Recovery = 141% Analysis Date = 07/21/14 Pct Recovery = 142% Analysis Date = 07/21/14 Pct Recovery = 142% Analysis Date = 07/16/14 Pct Recovery = 143% Analysis Date = 07/16/14 Pct Recovery = 143% Analysis Date = 07/11/14 Pct Recovery = 144% Analysis Date = 07/11/14 Pct Recovery = 144% Analysis Date = 07/07/14 Pct Recovery = 145% Analysis Date = 07/07/14 Pct Recovery = 145% Analysis Date = 07/02/14 Pct Recovery = 145% Analysis Date = 07/02/14 Pct Recovery = 145% Analysis Date = 06/27/14 Pct Recovery = 146% Analysis Date = 06/27/14 Pct Recovery = 146% Analysis Date = 06/22/14 Pct Recovery = 147% Analysis Date = 06/22/14 Pct Recovery = 147% Analysis Date = 06/17/14 Pct Recovery = 148% Analysis Date = 06/17/14 Pct Recovery = 148% Analysis Date = 06/13/14 Pct Recovery = 149% Analysis Date = 06/13/14 Pct Recovery = 149% Analysis Date = 06/08/14 Pct Recovery = 150% Analysis Date = 06/08/14 Pct Recovery = 150% Analysis Date = 06/03/14 Pct Recovery = 150% Analysis Date = 06/03/14 Pct Recovery = 150% Analysis Date = 05/29/14 Pct Recovery = 151% Analysis Date = 05/29/14 Pct Recovery = 151% Analysis Date = 05/24/14 Pct Recovery = 152% Analysis Date = 05/24/14 Pct Recovery = 152% Analysis Date = 05/20/14 Pct Recovery = 153% Analysis Date = 05/20/14 Pct Recovery = 153% Analysis Date = 05/15/14 Pct Recovery = 154% Analysis Date = 05/15/14 Pct Recovery = 154% Analysis Date = 05/10/14 Pct Recovery = 155% Analysis Date = 05/10/14 Pct Recovery = 155% Analysis Date = 05/05/14 Pct Recovery = 155% Analysis Date = 05/05/14 Pct Recovery = 155% Analysis Date = 05/01/14 Pct Recovery = 156% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
DICHLORODIFLUOROMETHANE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 50 89% 36% 73% 40%
Total 50 89% 36% 73% 40%

Sample Statistics
DICHLORODIFLUOROMETHANE

Characteristic N % % Basis
Plotted 50 100% Spiked
Estimated Values 50 100% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 50 .  
False Negatives 0 0% 0 out of 50
Not Spiked 23 .  
False Positives 0 0% 0 out of 23

BQS OBSP Determination:
DICHLOROFLUOROMETHANE
METHOD: 4440 , TESTIDCODE: 77119GCM66
Open Data Set

Analysis Date = 08/04/16 SpikeMix = Crescent 03FF058: 40 µl & Supelco LC20141V: 40 µl Pct Recovery = 110% Analysis Date = 07/20/16 SpikeMix = Supelco LC20141V: 40 µl & Accu 216041125: 40 µl Pct Recovery = 100% Analysis Date = 12/16/16 SpikeMix = NSI 041816AVOC: 40 µl & ChemService 5082900: 40 µl Pct Recovery = 108% Analysis Date = 11/21/16 SpikeMix = Crescent 03FF058: 25 µl & Supelco LC20141V: 25 µl Pct Recovery = 96% Analysis Date = 09/08/16 SpikeMix = Supelco LC20141V: 25 µl & Accu 216041125: 25 µl Pct Recovery = 108% Analysis Date = 08/31/16 SpikeMix = NSI 041816AVOC: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 110% Analysis Date = 08/12/16 SpikeMix = ChemService 5082900: 25 µl & Phenova B20160319: 25 µl Pct Recovery = 115% Analysis Date = 06/30/16 SpikeMix = Crescent 03FF058: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 110% Analysis Date = 03/19/15 SpikeMix = Spex Organics C1140417015: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 116% Analysis Date = 03/06/15 SpikeMix = ERA 0227-14-06.1A: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 88% Analysis Date = 12/17/14 SpikeMix = Supelco LC06438: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 94% Analysis Date = 11/22/14 SpikeMix = NSI 032614: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 108% Analysis Date = 09/21/14 SpikeMix = Supelco LC06438: 20 µl Pct Recovery = 103% Analysis Date = 08/19/14 SpikeMix = Spex Organics C1140417015: 20 µl & Accu 214031115: 20 µl Pct Recovery = 115% Analysis Date = 08/16/14 SpikeMix = ERA 0227-14-06.1A: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 123% Analysis Date = 06/10/14 SpikeMix = NSI 032614: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 103% Analysis Date = 09/29/15 SpikeMix = Accu 215041380: 25 µl & ERA 0406-15-03: 25 µl Pct Recovery = 96% Analysis Date = 08/15/15 SpikeMix = Supelco LC13545: 25 µl & Crescent 04EE008: 25 µl Pct Recovery = 100% Analysis Date = 07/13/15 SpikeMix = Crescent 04EE008: 25 µl & NSI 050515AVOC: 25 µl Pct Recovery = 98% Analysis Date = 10/13/16 SpikeMix = NSI 041816AVOC: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 93% Analysis Date = 05/27/16 SpikeMix = Phenova B20160319: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 97% Analysis Date = 11/29/16 SpikeMix = ChemService 5082900: 15 µl & Phenova B20160319: 15 µl Pct Recovery = 108% Analysis Date = 09/28/16 SpikeMix = Crescent 03FF058: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 103% Analysis Date = 06/30/16 SpikeMix = ChemService 5082900: 15 µl & Accu 216041125: 15 µl Pct Recovery = 107% Analysis Date = 06/10/16 SpikeMix = NSI 041816AVOC: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 104% Analysis Date = 04/02/16 SpikeMix = Supelco LC13545: 15 µl & Accu 215041380: 15 µl Pct Recovery = 99% Analysis Date = 03/04/16 SpikeMix = Accu 215041380: 15 µl & ERA 0406-15-03: 15 µl Pct Recovery = 97% Analysis Date = 06/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Accu 215041380: 15 µl Pct Recovery = 104% Analysis Date = 12/18/15 SpikeMix = Supelco LC13545: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 91% Analysis Date = 10/17/15 SpikeMix = Crescent 04EE008: 15 µl & NSI 050515AVOC: 15 µl Pct Recovery = 88% Analysis Date = 05/09/15 SpikeMix = Spex Organics EN150428007: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 95% Analysis Date = 11/06/14 SpikeMix = Spex Organics C1140417015: 10 µl & Crescent 03DD004: 10 µl Pct Recovery = 103% Analysis Date = 10/21/14 SpikeMix = ERA 0227-14-06.1A: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 93% Analysis Date = 09/09/14 SpikeMix = NSI 032614: 10 µl & Spex Organics C1140417015: 10 µl Pct Recovery = 119% Analysis Date = 07/23/14 SpikeMix = Spex Organics C1140417015: 10 µl & Accu 214031115: 10 µl Pct Recovery = 128% Analysis Date = 07/11/14 SpikeMix = Spex Organics C1140417015: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 109% Analysis Date = 06/18/14 SpikeMix = Supelco LC06438: 10 µl & Accu 214031115: 10 µl Pct Recovery = 102% Analysis Date = 05/03/14 SpikeMix = Crescent 03DD004: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 109% Analysis Date = 02/18/16 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 95% Analysis Date = 11/20/15 SpikeMix = Accu 215041380: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 102% Analysis Date = 11/12/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 107% Analysis Date = 05/21/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 103% Analysis Date = 05/13/16 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 100% Analysis Date = 01/27/16 SpikeMix = Crescent 04EE008: 10 µl & NSI 050515AVOC: 10 µl Pct Recovery = 107% Analysis Date = 07/31/15 SpikeMix = Crescent 04EE008: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 92% Analysis Date = 05/09/15 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 92% Analysis Date = 12/16/16 Pct Recovery = 106% Analysis Date = 12/11/16 Pct Recovery = 106% Analysis Date = 12/11/16 Pct Recovery = 106% Analysis Date = 12/06/16 Pct Recovery = 106% Analysis Date = 12/06/16 Pct Recovery = 106% Analysis Date = 12/01/16 Pct Recovery = 106% Analysis Date = 12/01/16 Pct Recovery = 106% Analysis Date = 11/26/16 Pct Recovery = 106% Analysis Date = 11/26/16 Pct Recovery = 106% Analysis Date = 11/22/16 Pct Recovery = 106% Analysis Date = 11/22/16 Pct Recovery = 106% Analysis Date = 11/17/16 Pct Recovery = 106% Analysis Date = 11/17/16 Pct Recovery = 106% Analysis Date = 11/12/16 Pct Recovery = 105% Analysis Date = 11/12/16 Pct Recovery = 105% Analysis Date = 11/07/16 Pct Recovery = 105% Analysis Date = 11/07/16 Pct Recovery = 105% Analysis Date = 11/02/16 Pct Recovery = 105% Analysis Date = 11/02/16 Pct Recovery = 105% Analysis Date = 10/29/16 Pct Recovery = 105% Analysis Date = 10/29/16 Pct Recovery = 105% Analysis Date = 10/24/16 Pct Recovery = 105% Analysis Date = 10/24/16 Pct Recovery = 105% Analysis Date = 10/19/16 Pct Recovery = 105% Analysis Date = 10/19/16 Pct Recovery = 105% Analysis Date = 10/14/16 Pct Recovery = 105% Analysis Date = 10/14/16 Pct Recovery = 105% Analysis Date = 10/09/16 Pct Recovery = 105% Analysis Date = 10/09/16 Pct Recovery = 105% Analysis Date = 10/05/16 Pct Recovery = 105% Analysis Date = 10/05/16 Pct Recovery = 105% Analysis Date = 09/30/16 Pct Recovery = 105% Analysis Date = 09/30/16 Pct Recovery = 105% Analysis Date = 09/25/16 Pct Recovery = 105% Analysis Date = 09/25/16 Pct Recovery = 105% Analysis Date = 09/20/16 Pct Recovery = 105% Analysis Date = 09/20/16 Pct Recovery = 105% Analysis Date = 09/15/16 Pct Recovery = 105% Analysis Date = 09/15/16 Pct Recovery = 105% Analysis Date = 09/11/16 Pct Recovery = 104% Analysis Date = 09/11/16 Pct Recovery = 104% Analysis Date = 09/06/16 Pct Recovery = 104% Analysis Date = 09/06/16 Pct Recovery = 104% Analysis Date = 09/01/16 Pct Recovery = 104% Analysis Date = 09/01/16 Pct Recovery = 104% Analysis Date = 08/27/16 Pct Recovery = 104% Analysis Date = 08/27/16 Pct Recovery = 104% Analysis Date = 08/23/16 Pct Recovery = 104% Analysis Date = 08/23/16 Pct Recovery = 104% Analysis Date = 08/18/16 Pct Recovery = 104% Analysis Date = 08/18/16 Pct Recovery = 104% Analysis Date = 08/13/16 Pct Recovery = 104% Analysis Date = 08/13/16 Pct Recovery = 104% Analysis Date = 08/08/16 Pct Recovery = 104% Analysis Date = 08/08/16 Pct Recovery = 104% Analysis Date = 08/03/16 Pct Recovery = 104% Analysis Date = 08/03/16 Pct Recovery = 104% Analysis Date = 07/30/16 Pct Recovery = 104% Analysis Date = 07/30/16 Pct Recovery = 104% Analysis Date = 07/25/16 Pct Recovery = 104% Analysis Date = 07/25/16 Pct Recovery = 104% Analysis Date = 07/20/16 Pct Recovery = 104% Analysis Date = 07/20/16 Pct Recovery = 104% Analysis Date = 07/15/16 Pct Recovery = 103% Analysis Date = 07/15/16 Pct Recovery = 103% Analysis Date = 07/10/16 Pct Recovery = 103% Analysis Date = 07/10/16 Pct Recovery = 103% Analysis Date = 07/06/16 Pct Recovery = 103% Analysis Date = 07/06/16 Pct Recovery = 103% Analysis Date = 07/01/16 Pct Recovery = 103% Analysis Date = 07/01/16 Pct Recovery = 103% Analysis Date = 06/26/16 Pct Recovery = 103% Analysis Date = 06/26/16 Pct Recovery = 103% Analysis Date = 06/21/16 Pct Recovery = 103% Analysis Date = 06/21/16 Pct Recovery = 103% Analysis Date = 06/16/16 Pct Recovery = 103% Analysis Date = 06/16/16 Pct Recovery = 103% Analysis Date = 06/12/16 Pct Recovery = 103% Analysis Date = 06/12/16 Pct Recovery = 103% Analysis Date = 06/07/16 Pct Recovery = 103% Analysis Date = 06/07/16 Pct Recovery = 103% Analysis Date = 06/02/16 Pct Recovery = 103% Analysis Date = 06/02/16 Pct Recovery = 103% Analysis Date = 05/28/16 Pct Recovery = 103% Analysis Date = 05/28/16 Pct Recovery = 103% Analysis Date = 05/24/16 Pct Recovery = 102% Analysis Date = 05/24/16 Pct Recovery = 102% Analysis Date = 05/19/16 Pct Recovery = 102% Analysis Date = 05/19/16 Pct Recovery = 102% Analysis Date = 05/14/16 Pct Recovery = 102% Analysis Date = 05/14/16 Pct Recovery = 102% Analysis Date = 05/09/16 Pct Recovery = 102% Analysis Date = 05/09/16 Pct Recovery = 102% Analysis Date = 05/04/16 Pct Recovery = 102% Analysis Date = 05/04/16 Pct Recovery = 102% Analysis Date = 04/30/16 Pct Recovery = 102% Analysis Date = 04/30/16 Pct Recovery = 102% Analysis Date = 04/25/16 Pct Recovery = 102% Analysis Date = 04/25/16 Pct Recovery = 102% Analysis Date = 04/20/16 Pct Recovery = 102% Analysis Date = 04/20/16 Pct Recovery = 102% Analysis Date = 04/15/16 Pct Recovery = 102% Analysis Date = 04/15/16 Pct Recovery = 102% Analysis Date = 04/10/16 Pct Recovery = 101% Analysis Date = 04/10/16 Pct Recovery = 101% Analysis Date = 04/06/16 Pct Recovery = 101% Analysis Date = 04/06/16 Pct Recovery = 101% Analysis Date = 04/01/16 Pct Recovery = 101% Analysis Date = 04/01/16 Pct Recovery = 101% Analysis Date = 03/27/16 Pct Recovery = 101% Analysis Date = 03/27/16 Pct Recovery = 101% Analysis Date = 03/22/16 Pct Recovery = 101% Analysis Date = 03/22/16 Pct Recovery = 101% Analysis Date = 03/17/16 Pct Recovery = 101% Analysis Date = 03/17/16 Pct Recovery = 101% Analysis Date = 03/13/16 Pct Recovery = 101% Analysis Date = 03/13/16 Pct Recovery = 101% Analysis Date = 03/08/16 Pct Recovery = 101% Analysis Date = 03/08/16 Pct Recovery = 101% Analysis Date = 03/03/16 Pct Recovery = 101% Analysis Date = 03/03/16 Pct Recovery = 101% Analysis Date = 02/27/16 Pct Recovery = 100% Analysis Date = 02/27/16 Pct Recovery = 100% Analysis Date = 02/23/16 Pct Recovery = 100% Analysis Date = 02/23/16 Pct Recovery = 100% Analysis Date = 02/18/16 Pct Recovery = 100% Analysis Date = 02/18/16 Pct Recovery = 100% Analysis Date = 02/13/16 Pct Recovery = 100% Analysis Date = 02/13/16 Pct Recovery = 100% Analysis Date = 02/08/16 Pct Recovery = 100% Analysis Date = 02/08/16 Pct Recovery = 100% Analysis Date = 02/03/16 Pct Recovery = 100% Analysis Date = 02/03/16 Pct Recovery = 100% Analysis Date = 01/30/16 Pct Recovery = 100% Analysis Date = 01/30/16 Pct Recovery = 100% Analysis Date = 01/25/16 Pct Recovery = 100% Analysis Date = 01/25/16 Pct Recovery = 100% Analysis Date = 01/20/16 Pct Recovery = 100% Analysis Date = 01/20/16 Pct Recovery = 100% Analysis Date = 01/15/16 Pct Recovery = 100% Analysis Date = 01/15/16 Pct Recovery = 100% Analysis Date = 01/10/16 Pct Recovery = 99% Analysis Date = 01/10/16 Pct Recovery = 99% Analysis Date = 01/06/16 Pct Recovery = 99% Analysis Date = 01/06/16 Pct Recovery = 99% Analysis Date = 01/01/16 Pct Recovery = 99% Analysis Date = 01/01/16 Pct Recovery = 99% Analysis Date = 12/27/15 Pct Recovery = 99% Analysis Date = 12/27/15 Pct Recovery = 99% Analysis Date = 12/22/15 Pct Recovery = 99% Analysis Date = 12/22/15 Pct Recovery = 99% Analysis Date = 12/17/15 Pct Recovery = 99% Analysis Date = 12/17/15 Pct Recovery = 99% Analysis Date = 12/13/15 Pct Recovery = 99% Analysis Date = 12/13/15 Pct Recovery = 99% Analysis Date = 12/08/15 Pct Recovery = 99% Analysis Date = 12/08/15 Pct Recovery = 99% Analysis Date = 12/03/15 Pct Recovery = 99% Analysis Date = 12/03/15 Pct Recovery = 99% Analysis Date = 11/28/15 Pct Recovery = 99% Analysis Date = 11/28/15 Pct Recovery = 99% Analysis Date = 11/24/15 Pct Recovery = 99% Analysis Date = 11/24/15 Pct Recovery = 99% Analysis Date = 11/19/15 Pct Recovery = 98% Analysis Date = 11/19/15 Pct Recovery = 98% Analysis Date = 11/14/15 Pct Recovery = 98% Analysis Date = 11/14/15 Pct Recovery = 98% Analysis Date = 11/09/15 Pct Recovery = 98% Analysis Date = 11/09/15 Pct Recovery = 98% Analysis Date = 11/04/15 Pct Recovery = 98% Analysis Date = 11/04/15 Pct Recovery = 98% Analysis Date = 10/31/15 Pct Recovery = 98% Analysis Date = 10/31/15 Pct Recovery = 98% Analysis Date = 10/26/15 Pct Recovery = 98% Analysis Date = 10/26/15 Pct Recovery = 98% Analysis Date = 10/21/15 Pct Recovery = 98% Analysis Date = 10/21/15 Pct Recovery = 98% Analysis Date = 10/16/15 Pct Recovery = 98% Analysis Date = 10/16/15 Pct Recovery = 98% Analysis Date = 10/11/15 Pct Recovery = 98% Analysis Date = 10/11/15 Pct Recovery = 98% Analysis Date = 10/07/15 Pct Recovery = 98% Analysis Date = 10/07/15 Pct Recovery = 98% Analysis Date = 10/02/15 Pct Recovery = 98% Analysis Date = 10/02/15 Pct Recovery = 98% Analysis Date = 09/27/15 Pct Recovery = 98% Analysis Date = 09/27/15 Pct Recovery = 98% Analysis Date = 09/22/15 Pct Recovery = 98% Analysis Date = 09/22/15 Pct Recovery = 98% Analysis Date = 09/17/15 Pct Recovery = 98% Analysis Date = 09/17/15 Pct Recovery = 98% Analysis Date = 09/13/15 Pct Recovery = 98% Analysis Date = 09/13/15 Pct Recovery = 98% Analysis Date = 09/08/15 Pct Recovery = 98% Analysis Date = 09/08/15 Pct Recovery = 98% Analysis Date = 09/03/15 Pct Recovery = 98% Analysis Date = 09/03/15 Pct Recovery = 98% Analysis Date = 08/29/15 Pct Recovery = 98% Analysis Date = 08/29/15 Pct Recovery = 98% Analysis Date = 08/25/15 Pct Recovery = 98% Analysis Date = 08/25/15 Pct Recovery = 98% Analysis Date = 08/20/15 Pct Recovery = 98% Analysis Date = 08/20/15 Pct Recovery = 98% Analysis Date = 08/15/15 Pct Recovery = 99% Analysis Date = 08/15/15 Pct Recovery = 99% Analysis Date = 08/10/15 Pct Recovery = 99% Analysis Date = 08/10/15 Pct Recovery = 99% Analysis Date = 08/05/15 Pct Recovery = 99% Analysis Date = 08/05/15 Pct Recovery = 99% Analysis Date = 08/01/15 Pct Recovery = 99% Analysis Date = 08/01/15 Pct Recovery = 99% Analysis Date = 07/27/15 Pct Recovery = 99% Analysis Date = 07/27/15 Pct Recovery = 99% Analysis Date = 07/22/15 Pct Recovery = 99% Analysis Date = 07/22/15 Pct Recovery = 99% Analysis Date = 07/17/15 Pct Recovery = 99% Analysis Date = 07/17/15 Pct Recovery = 99% Analysis Date = 07/12/15 Pct Recovery = 99% Analysis Date = 07/12/15 Pct Recovery = 99% Analysis Date = 07/08/15 Pct Recovery = 99% Analysis Date = 07/08/15 Pct Recovery = 99% Analysis Date = 07/03/15 Pct Recovery = 99% Analysis Date = 07/03/15 Pct Recovery = 99% Analysis Date = 06/28/15 Pct Recovery = 99% Analysis Date = 06/28/15 Pct Recovery = 99% Analysis Date = 06/23/15 Pct Recovery = 99% Analysis Date = 06/23/15 Pct Recovery = 99% Analysis Date = 06/18/15 Pct Recovery = 99% Analysis Date = 06/18/15 Pct Recovery = 99% Analysis Date = 06/14/15 Pct Recovery = 99% Analysis Date = 06/14/15 Pct Recovery = 99% Analysis Date = 06/09/15 Pct Recovery = 99% Analysis Date = 06/09/15 Pct Recovery = 99% Analysis Date = 06/04/15 Pct Recovery = 99% Analysis Date = 06/04/15 Pct Recovery = 99% Analysis Date = 05/30/15 Pct Recovery = 99% Analysis Date = 05/30/15 Pct Recovery = 99% Analysis Date = 05/25/15 Pct Recovery = 99% Analysis Date = 05/25/15 Pct Recovery = 99% Analysis Date = 05/21/15 Pct Recovery = 99% Analysis Date = 05/21/15 Pct Recovery = 99% Analysis Date = 05/16/15 Pct Recovery = 99% Analysis Date = 05/16/15 Pct Recovery = 99% Analysis Date = 05/11/15 Pct Recovery = 99% Analysis Date = 05/11/15 Pct Recovery = 99% Analysis Date = 05/06/15 Pct Recovery = 99% Analysis Date = 05/06/15 Pct Recovery = 99% Analysis Date = 05/02/15 Pct Recovery = 99% Analysis Date = 05/02/15 Pct Recovery = 99% Analysis Date = 04/27/15 Pct Recovery = 100% Analysis Date = 04/27/15 Pct Recovery = 100% Analysis Date = 04/22/15 Pct Recovery = 100% Analysis Date = 04/22/15 Pct Recovery = 100% Analysis Date = 04/17/15 Pct Recovery = 100% Analysis Date = 04/17/15 Pct Recovery = 100% Analysis Date = 04/12/15 Pct Recovery = 100% Analysis Date = 04/12/15 Pct Recovery = 100% Analysis Date = 04/08/15 Pct Recovery = 100% Analysis Date = 04/08/15 Pct Recovery = 100% Analysis Date = 04/03/15 Pct Recovery = 100% Analysis Date = 04/03/15 Pct Recovery = 100% Analysis Date = 03/29/15 Pct Recovery = 101% Analysis Date = 03/29/15 Pct Recovery = 101% Analysis Date = 03/24/15 Pct Recovery = 101% Analysis Date = 03/24/15 Pct Recovery = 101% Analysis Date = 03/19/15 Pct Recovery = 101% Analysis Date = 03/19/15 Pct Recovery = 101% Analysis Date = 03/15/15 Pct Recovery = 101% Analysis Date = 03/15/15 Pct Recovery = 101% Analysis Date = 03/10/15 Pct Recovery = 101% Analysis Date = 03/10/15 Pct Recovery = 101% Analysis Date = 03/05/15 Pct Recovery = 101% Analysis Date = 03/05/15 Pct Recovery = 101% Analysis Date = 02/28/15 Pct Recovery = 102% Analysis Date = 02/28/15 Pct Recovery = 102% Analysis Date = 02/23/15 Pct Recovery = 102% Analysis Date = 02/23/15 Pct Recovery = 102% Analysis Date = 02/19/15 Pct Recovery = 102% Analysis Date = 02/19/15 Pct Recovery = 102% Analysis Date = 02/14/15 Pct Recovery = 102% Analysis Date = 02/14/15 Pct Recovery = 102% Analysis Date = 02/09/15 Pct Recovery = 102% Analysis Date = 02/09/15 Pct Recovery = 102% Analysis Date = 02/04/15 Pct Recovery = 102% Analysis Date = 02/04/15 Pct Recovery = 102% Analysis Date = 01/31/15 Pct Recovery = 103% Analysis Date = 01/31/15 Pct Recovery = 103% Analysis Date = 01/26/15 Pct Recovery = 103% Analysis Date = 01/26/15 Pct Recovery = 103% Analysis Date = 01/21/15 Pct Recovery = 103% Analysis Date = 01/21/15 Pct Recovery = 103% Analysis Date = 01/16/15 Pct Recovery = 103% Analysis Date = 01/16/15 Pct Recovery = 103% Analysis Date = 01/11/15 Pct Recovery = 103% Analysis Date = 01/11/15 Pct Recovery = 103% Analysis Date = 01/07/15 Pct Recovery = 104% Analysis Date = 01/07/15 Pct Recovery = 104% Analysis Date = 01/02/15 Pct Recovery = 104% Analysis Date = 01/02/15 Pct Recovery = 104% Analysis Date = 12/28/14 Pct Recovery = 104% Analysis Date = 12/28/14 Pct Recovery = 104% Analysis Date = 12/23/14 Pct Recovery = 104% Analysis Date = 12/23/14 Pct Recovery = 104% Analysis Date = 12/18/14 Pct Recovery = 104% Analysis Date = 12/18/14 Pct Recovery = 104% Analysis Date = 12/14/14 Pct Recovery = 105% Analysis Date = 12/14/14 Pct Recovery = 105% Analysis Date = 12/09/14 Pct Recovery = 105% Analysis Date = 12/09/14 Pct Recovery = 105% Analysis Date = 12/04/14 Pct Recovery = 105% Analysis Date = 12/04/14 Pct Recovery = 105% Analysis Date = 11/29/14 Pct Recovery = 105% Analysis Date = 11/29/14 Pct Recovery = 105% Analysis Date = 11/24/14 Pct Recovery = 105% Analysis Date = 11/24/14 Pct Recovery = 105% Analysis Date = 11/20/14 Pct Recovery = 105% Analysis Date = 11/20/14 Pct Recovery = 105% Analysis Date = 11/15/14 Pct Recovery = 106% Analysis Date = 11/15/14 Pct Recovery = 106% Analysis Date = 11/10/14 Pct Recovery = 106% Analysis Date = 11/10/14 Pct Recovery = 106% Analysis Date = 11/05/14 Pct Recovery = 106% Analysis Date = 11/05/14 Pct Recovery = 106% Analysis Date = 11/01/14 Pct Recovery = 106% Analysis Date = 11/01/14 Pct Recovery = 106% Analysis Date = 10/27/14 Pct Recovery = 106% Analysis Date = 10/27/14 Pct Recovery = 106% Analysis Date = 10/22/14 Pct Recovery = 106% Analysis Date = 10/22/14 Pct Recovery = 106% Analysis Date = 10/17/14 Pct Recovery = 107% Analysis Date = 10/17/14 Pct Recovery = 107% Analysis Date = 10/12/14 Pct Recovery = 107% Analysis Date = 10/12/14 Pct Recovery = 107% Analysis Date = 10/08/14 Pct Recovery = 107% Analysis Date = 10/08/14 Pct Recovery = 107% Analysis Date = 10/03/14 Pct Recovery = 107% Analysis Date = 10/03/14 Pct Recovery = 107% Analysis Date = 09/28/14 Pct Recovery = 107% Analysis Date = 09/28/14 Pct Recovery = 107% Analysis Date = 09/23/14 Pct Recovery = 108% Analysis Date = 09/23/14 Pct Recovery = 108% Analysis Date = 09/18/14 Pct Recovery = 108% Analysis Date = 09/18/14 Pct Recovery = 108% Analysis Date = 09/14/14 Pct Recovery = 108% Analysis Date = 09/14/14 Pct Recovery = 108% Analysis Date = 09/09/14 Pct Recovery = 108% Analysis Date = 09/09/14 Pct Recovery = 108% Analysis Date = 09/04/14 Pct Recovery = 108% Analysis Date = 09/04/14 Pct Recovery = 108% Analysis Date = 08/30/14 Pct Recovery = 108% Analysis Date = 08/30/14 Pct Recovery = 108% Analysis Date = 08/25/14 Pct Recovery = 109% Analysis Date = 08/25/14 Pct Recovery = 109% Analysis Date = 08/21/14 Pct Recovery = 109% Analysis Date = 08/21/14 Pct Recovery = 109% Analysis Date = 08/16/14 Pct Recovery = 109% Analysis Date = 08/16/14 Pct Recovery = 109% Analysis Date = 08/11/14 Pct Recovery = 109% Analysis Date = 08/11/14 Pct Recovery = 109% Analysis Date = 08/06/14 Pct Recovery = 109% Analysis Date = 08/06/14 Pct Recovery = 109% Analysis Date = 08/02/14 Pct Recovery = 110% Analysis Date = 08/02/14 Pct Recovery = 110% Analysis Date = 07/28/14 Pct Recovery = 110% Analysis Date = 07/28/14 Pct Recovery = 110% Analysis Date = 07/23/14 Pct Recovery = 110% Analysis Date = 07/23/14 Pct Recovery = 110% Analysis Date = 07/18/14 Pct Recovery = 110% Analysis Date = 07/18/14 Pct Recovery = 110% Analysis Date = 07/13/14 Pct Recovery = 110% Analysis Date = 07/13/14 Pct Recovery = 110% Analysis Date = 07/09/14 Pct Recovery = 111% Analysis Date = 07/09/14 Pct Recovery = 111% Analysis Date = 07/04/14 Pct Recovery = 111% Analysis Date = 07/04/14 Pct Recovery = 111% Analysis Date = 06/29/14 Pct Recovery = 111% Analysis Date = 06/29/14 Pct Recovery = 111% Analysis Date = 06/24/14 Pct Recovery = 111% Analysis Date = 06/24/14 Pct Recovery = 111% Analysis Date = 06/19/14 Pct Recovery = 111% Analysis Date = 06/19/14 Pct Recovery = 111% Analysis Date = 06/15/14 Pct Recovery = 111% Analysis Date = 06/15/14 Pct Recovery = 111% Analysis Date = 06/10/14 Pct Recovery = 112% Analysis Date = 06/10/14 Pct Recovery = 112% Analysis Date = 06/05/14 Pct Recovery = 112% Analysis Date = 06/05/14 Pct Recovery = 112% Analysis Date = 05/31/14 Pct Recovery = 112% Analysis Date = 05/31/14 Pct Recovery = 112% Analysis Date = 05/26/14 Pct Recovery = 112% Analysis Date = 05/26/14 Pct Recovery = 112% Analysis Date = 05/22/14 Pct Recovery = 112% Analysis Date = 05/22/14 Pct Recovery = 112% Analysis Date = 05/17/14 Pct Recovery = 113% Analysis Date = 05/17/14 Pct Recovery = 113% Analysis Date = 05/12/14 Pct Recovery = 113% Analysis Date = 05/12/14 Pct Recovery = 113% Analysis Date = 05/07/14 Pct Recovery = 113% Analysis Date = 05/07/14 Pct Recovery = 113% Analysis Date = 05/03/14 Pct Recovery = 113% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
DICHLOROFLUOROMETHANE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 46 103% 9% 103% 9%
Total 46 103% 9% 103% 9%

Sample Statistics
DICHLOROFLUOROMETHANE

Characteristic N % % Basis
Plotted 46 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 46 .  
False Negatives 0 0% 0 out of 46
Not Spiked 26 .  
False Positives 0 0% 0 out of 26

BQS OBSP Determination:
DICHLOROMETHANE
METHOD: 4440 , TESTIDCODE: 34423GCM66
Open Data Set

Analysis Date = 12/12/16 SpikeMix = Accu 216041125: 40 µl & Crescent 03FF058: 40 µl Pct Recovery = 125% Analysis Date = 07/20/16 SpikeMix = Supelco LC20141V: 40 µl & Accu 216041125: 40 µl Pct Recovery = 121% Analysis Date = 07/14/16 SpikeMix = Accu 216041125: 40 µl & NSI 041816AVOC: 40 µl Pct Recovery = 163% Analysis Date = 08/12/16 SpikeMix = ChemService 5082900: 25 µl & Phenova B20160319: 25 µl Pct Recovery = 113% Analysis Date = 06/21/16 SpikeMix = Phenova B20160319: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 107% Analysis Date = 09/08/16 SpikeMix = Supelco LC20141V: 25 µl & Accu 216041125: 25 µl Pct Recovery = 121% Analysis Date = 05/24/16 SpikeMix = Accu 216041125: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 121% Analysis Date = 03/06/15 SpikeMix = ERA 0227-14-06.1A: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 100% Analysis Date = 12/17/14 SpikeMix = Supelco LC06438: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 106% Analysis Date = 09/21/14 SpikeMix = Supelco LC06438: 20 µl Pct Recovery = 106% Analysis Date = 06/10/14 SpikeMix = NSI 032614: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 118% Analysis Date = 03/19/15 SpikeMix = Spex Organics C1140417015: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 125% Analysis Date = 11/22/14 SpikeMix = NSI 032614: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 119% Analysis Date = 08/19/14 SpikeMix = Spex Organics C1140417015: 20 µl & Accu 214031115: 20 µl Pct Recovery = 125% Analysis Date = 08/16/14 SpikeMix = ERA 0227-14-06.1A: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 119% Analysis Date = 09/29/15 SpikeMix = Accu 215041380: 25 µl & ERA 0406-15-03: 25 µl Pct Recovery = 87% Analysis Date = 08/15/15 SpikeMix = Supelco LC13545: 25 µl & Crescent 04EE008: 25 µl Pct Recovery = 107% Analysis Date = 07/13/15 SpikeMix = Crescent 04EE008: 25 µl & NSI 050515AVOC: 25 µl Pct Recovery = 120% Analysis Date = 11/29/16 SpikeMix = ChemService 5082900: 15 µl & Phenova B20160319: 15 µl Pct Recovery = 109% Analysis Date = 09/08/16 SpikeMix = Phenova B20160319: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 109% Analysis Date = 07/29/16 SpikeMix = Phenova B20160319: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 159% Analysis Date = 05/27/16 SpikeMix = Phenova B20160319: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 129% Analysis Date = 10/13/16 SpikeMix = Accu 216041125: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 181% Analysis Date = 08/20/16 SpikeMix = Accu 216041125: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 141% Analysis Date = 06/30/16 SpikeMix = ChemService 5082900: 15 µl & Accu 216041125: 15 µl Pct Recovery = 101% Analysis Date = 04/02/16 SpikeMix = Supelco LC13545: 15 µl & Accu 215041380: 15 µl Pct Recovery = 100% Analysis Date = 03/04/16 SpikeMix = Accu 215041380: 15 µl & ERA 0406-15-03: 15 µl Pct Recovery = 89% Analysis Date = 06/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Accu 215041380: 15 µl Pct Recovery = 111% Analysis Date = 12/18/15 SpikeMix = Supelco LC13545: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 111% Analysis Date = 10/17/15 SpikeMix = Crescent 04EE008: 15 µl & NSI 050515AVOC: 15 µl Pct Recovery = 111% Analysis Date = 05/09/15 SpikeMix = Spex Organics EN150428007: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 100% Analysis Date = 10/21/14 SpikeMix = ERA 0227-14-06.1A: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 100% Analysis Date = 06/18/14 SpikeMix = Supelco LC06438: 10 µl & Accu 214031115: 10 µl Pct Recovery = 112% Analysis Date = 05/30/14 SpikeMix = NSI 032614: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 100% Analysis Date = 05/03/14 SpikeMix = Crescent 03DD004: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 100% Analysis Date = 11/06/14 SpikeMix = Spex Organics C1140417015: 10 µl & Crescent 03DD004: 10 µl Pct Recovery = 113% Analysis Date = 09/09/14 SpikeMix = NSI 032614: 10 µl & Spex Organics C1140417015: 10 µl Pct Recovery = 125% Analysis Date = 07/23/14 SpikeMix = Spex Organics C1140417015: 10 µl & Accu 214031115: 10 µl Pct Recovery = 113% Analysis Date = 07/11/14 SpikeMix = Spex Organics C1140417015: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 100% Analysis Date = 02/18/16 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 100% Analysis Date = 11/20/15 SpikeMix = Accu 215041380: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 100% Analysis Date = 11/12/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 100% Analysis Date = 05/21/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 100% Analysis Date = 05/13/16 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 117% Analysis Date = 01/27/16 SpikeMix = Crescent 04EE008: 10 µl & NSI 050515AVOC: 10 µl Pct Recovery = 117% Analysis Date = 07/31/15 SpikeMix = Crescent 04EE008: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 117% Analysis Date = 05/09/15 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 117% Analysis Date = 12/12/16 Pct Recovery = 138% Analysis Date = 12/07/16 Pct Recovery = 137% Analysis Date = 12/07/16 Pct Recovery = 137% Analysis Date = 12/02/16 Pct Recovery = 137% Analysis Date = 12/02/16 Pct Recovery = 137% Analysis Date = 11/27/16 Pct Recovery = 137% Analysis Date = 11/27/16 Pct Recovery = 137% Analysis Date = 11/22/16 Pct Recovery = 136% Analysis Date = 11/22/16 Pct Recovery = 136% Analysis Date = 11/18/16 Pct Recovery = 136% Analysis Date = 11/18/16 Pct Recovery = 136% Analysis Date = 11/13/16 Pct Recovery = 135% Analysis Date = 11/13/16 Pct Recovery = 135% Analysis Date = 11/08/16 Pct Recovery = 135% Analysis Date = 11/08/16 Pct Recovery = 135% Analysis Date = 11/03/16 Pct Recovery = 134% Analysis Date = 11/03/16 Pct Recovery = 134% Analysis Date = 10/30/16 Pct Recovery = 134% Analysis Date = 10/30/16 Pct Recovery = 134% Analysis Date = 10/25/16 Pct Recovery = 133% Analysis Date = 10/25/16 Pct Recovery = 133% Analysis Date = 10/20/16 Pct Recovery = 133% Analysis Date = 10/20/16 Pct Recovery = 133% Analysis Date = 10/15/16 Pct Recovery = 133% Analysis Date = 10/15/16 Pct Recovery = 133% Analysis Date = 10/10/16 Pct Recovery = 132% Analysis Date = 10/10/16 Pct Recovery = 132% Analysis Date = 10/06/16 Pct Recovery = 132% Analysis Date = 10/06/16 Pct Recovery = 132% Analysis Date = 10/01/16 Pct Recovery = 131% Analysis Date = 10/01/16 Pct Recovery = 131% Analysis Date = 09/26/16 Pct Recovery = 131% Analysis Date = 09/26/16 Pct Recovery = 131% Analysis Date = 09/21/16 Pct Recovery = 130% Analysis Date = 09/21/16 Pct Recovery = 130% Analysis Date = 09/17/16 Pct Recovery = 130% Analysis Date = 09/17/16 Pct Recovery = 130% Analysis Date = 09/12/16 Pct Recovery = 129% Analysis Date = 09/12/16 Pct Recovery = 129% Analysis Date = 09/07/16 Pct Recovery = 129% Analysis Date = 09/07/16 Pct Recovery = 129% Analysis Date = 09/02/16 Pct Recovery = 129% Analysis Date = 09/02/16 Pct Recovery = 129% Analysis Date = 08/29/16 Pct Recovery = 128% Analysis Date = 08/29/16 Pct Recovery = 128% Analysis Date = 08/24/16 Pct Recovery = 128% Analysis Date = 08/24/16 Pct Recovery = 128% Analysis Date = 08/19/16 Pct Recovery = 127% Analysis Date = 08/19/16 Pct Recovery = 127% Analysis Date = 08/14/16 Pct Recovery = 127% Analysis Date = 08/14/16 Pct Recovery = 127% Analysis Date = 08/09/16 Pct Recovery = 126% Analysis Date = 08/09/16 Pct Recovery = 126% Analysis Date = 08/05/16 Pct Recovery = 126% Analysis Date = 08/05/16 Pct Recovery = 126% Analysis Date = 07/31/16 Pct Recovery = 125% Analysis Date = 07/31/16 Pct Recovery = 125% Analysis Date = 07/26/16 Pct Recovery = 125% Analysis Date = 07/26/16 Pct Recovery = 125% Analysis Date = 07/21/16 Pct Recovery = 125% Analysis Date = 07/21/16 Pct Recovery = 125% Analysis Date = 07/17/16 Pct Recovery = 124% Analysis Date = 07/17/16 Pct Recovery = 124% Analysis Date = 07/12/16 Pct Recovery = 124% Analysis Date = 07/12/16 Pct Recovery = 124% Analysis Date = 07/07/16 Pct Recovery = 123% Analysis Date = 07/07/16 Pct Recovery = 123% Analysis Date = 07/02/16 Pct Recovery = 123% Analysis Date = 07/02/16 Pct Recovery = 123% Analysis Date = 06/28/16 Pct Recovery = 122% Analysis Date = 06/28/16 Pct Recovery = 122% Analysis Date = 06/23/16 Pct Recovery = 122% Analysis Date = 06/23/16 Pct Recovery = 122% Analysis Date = 06/18/16 Pct Recovery = 122% Analysis Date = 06/18/16 Pct Recovery = 122% Analysis Date = 06/13/16 Pct Recovery = 121% Analysis Date = 06/13/16 Pct Recovery = 121% Analysis Date = 06/08/16 Pct Recovery = 121% Analysis Date = 06/08/16 Pct Recovery = 121% Analysis Date = 06/04/16 Pct Recovery = 120% Analysis Date = 06/04/16 Pct Recovery = 120% Analysis Date = 05/30/16 Pct Recovery = 120% Analysis Date = 05/30/16 Pct Recovery = 120% Analysis Date = 05/25/16 Pct Recovery = 119% Analysis Date = 05/25/16 Pct Recovery = 119% Analysis Date = 05/20/16 Pct Recovery = 119% Analysis Date = 05/20/16 Pct Recovery = 119% Analysis Date = 05/16/16 Pct Recovery = 119% Analysis Date = 05/16/16 Pct Recovery = 119% Analysis Date = 05/11/16 Pct Recovery = 118% Analysis Date = 05/11/16 Pct Recovery = 118% Analysis Date = 05/06/16 Pct Recovery = 118% Analysis Date = 05/06/16 Pct Recovery = 118% Analysis Date = 05/01/16 Pct Recovery = 117% Analysis Date = 05/01/16 Pct Recovery = 117% Analysis Date = 04/27/16 Pct Recovery = 117% Analysis Date = 04/27/16 Pct Recovery = 117% Analysis Date = 04/22/16 Pct Recovery = 116% Analysis Date = 04/22/16 Pct Recovery = 116% Analysis Date = 04/17/16 Pct Recovery = 116% Analysis Date = 04/17/16 Pct Recovery = 116% Analysis Date = 04/12/16 Pct Recovery = 116% Analysis Date = 04/12/16 Pct Recovery = 116% Analysis Date = 04/07/16 Pct Recovery = 115% Analysis Date = 04/07/16 Pct Recovery = 115% Analysis Date = 04/03/16 Pct Recovery = 115% Analysis Date = 04/03/16 Pct Recovery = 115% Analysis Date = 03/29/16 Pct Recovery = 114% Analysis Date = 03/29/16 Pct Recovery = 114% Analysis Date = 03/24/16 Pct Recovery = 114% Analysis Date = 03/24/16 Pct Recovery = 114% Analysis Date = 03/19/16 Pct Recovery = 113% Analysis Date = 03/19/16 Pct Recovery = 113% Analysis Date = 03/15/16 Pct Recovery = 113% Analysis Date = 03/15/16 Pct Recovery = 113% Analysis Date = 03/10/16 Pct Recovery = 113% Analysis Date = 03/10/16 Pct Recovery = 113% Analysis Date = 03/05/16 Pct Recovery = 112% Analysis Date = 03/05/16 Pct Recovery = 112% Analysis Date = 02/29/16 Pct Recovery = 112% Analysis Date = 02/29/16 Pct Recovery = 112% Analysis Date = 02/25/16 Pct Recovery = 111% Analysis Date = 02/25/16 Pct Recovery = 111% Analysis Date = 02/20/16 Pct Recovery = 111% Analysis Date = 02/20/16 Pct Recovery = 111% Analysis Date = 02/15/16 Pct Recovery = 111% Analysis Date = 02/15/16 Pct Recovery = 111% Analysis Date = 02/10/16 Pct Recovery = 110% Analysis Date = 02/10/16 Pct Recovery = 110% Analysis Date = 02/05/16 Pct Recovery = 110% Analysis Date = 02/05/16 Pct Recovery = 110% Analysis Date = 02/01/16 Pct Recovery = 110% Analysis Date = 02/01/16 Pct Recovery = 110% Analysis Date = 01/27/16 Pct Recovery = 110% Analysis Date = 01/27/16 Pct Recovery = 110% Analysis Date = 01/22/16 Pct Recovery = 109% Analysis Date = 01/22/16 Pct Recovery = 109% Analysis Date = 01/17/16 Pct Recovery = 109% Analysis Date = 01/17/16 Pct Recovery = 109% Analysis Date = 01/13/16 Pct Recovery = 109% Analysis Date = 01/13/16 Pct Recovery = 109% Analysis Date = 01/08/16 Pct Recovery = 109% Analysis Date = 01/08/16 Pct Recovery = 109% Analysis Date = 01/03/16 Pct Recovery = 109% Analysis Date = 01/03/16 Pct Recovery = 109% Analysis Date = 12/29/15 Pct Recovery = 108% Analysis Date = 12/29/15 Pct Recovery = 108% Analysis Date = 12/25/15 Pct Recovery = 108% Analysis Date = 12/25/15 Pct Recovery = 108% Analysis Date = 12/20/15 Pct Recovery = 108% Analysis Date = 12/20/15 Pct Recovery = 108% Analysis Date = 12/15/15 Pct Recovery = 108% Analysis Date = 12/15/15 Pct Recovery = 108% Analysis Date = 12/10/15 Pct Recovery = 107% Analysis Date = 12/10/15 Pct Recovery = 107% Analysis Date = 12/05/15 Pct Recovery = 107% Analysis Date = 12/05/15 Pct Recovery = 107% Analysis Date = 12/01/15 Pct Recovery = 107% Analysis Date = 12/01/15 Pct Recovery = 107% Analysis Date = 11/26/15 Pct Recovery = 107% Analysis Date = 11/26/15 Pct Recovery = 107% Analysis Date = 11/21/15 Pct Recovery = 106% Analysis Date = 11/21/15 Pct Recovery = 106% Analysis Date = 11/16/15 Pct Recovery = 106% Analysis Date = 11/16/15 Pct Recovery = 106% Analysis Date = 11/12/15 Pct Recovery = 106% Analysis Date = 11/12/15 Pct Recovery = 106% Analysis Date = 11/07/15 Pct Recovery = 106% Analysis Date = 11/07/15 Pct Recovery = 106% Analysis Date = 11/02/15 Pct Recovery = 107% Analysis Date = 11/02/15 Pct Recovery = 107% Analysis Date = 10/28/15 Pct Recovery = 107% Analysis Date = 10/28/15 Pct Recovery = 107% Analysis Date = 10/24/15 Pct Recovery = 107% Analysis Date = 10/24/15 Pct Recovery = 107% Analysis Date = 10/19/15 Pct Recovery = 107% Analysis Date = 10/19/15 Pct Recovery = 107% Analysis Date = 10/14/15 Pct Recovery = 107% Analysis Date = 10/14/15 Pct Recovery = 107% Analysis Date = 10/09/15 Pct Recovery = 107% Analysis Date = 10/09/15 Pct Recovery = 107% Analysis Date = 10/04/15 Pct Recovery = 107% Analysis Date = 10/04/15 Pct Recovery = 107% Analysis Date = 09/30/15 Pct Recovery = 107% Analysis Date = 09/30/15 Pct Recovery = 107% Analysis Date = 09/25/15 Pct Recovery = 107% Analysis Date = 09/25/15 Pct Recovery = 107% Analysis Date = 09/20/15 Pct Recovery = 107% Analysis Date = 09/20/15 Pct Recovery = 107% Analysis Date = 09/15/15 Pct Recovery = 107% Analysis Date = 09/15/15 Pct Recovery = 107% Analysis Date = 09/11/15 Pct Recovery = 107% Analysis Date = 09/11/15 Pct Recovery = 107% Analysis Date = 09/06/15 Pct Recovery = 107% Analysis Date = 09/06/15 Pct Recovery = 107% Analysis Date = 09/01/15 Pct Recovery = 107% Analysis Date = 09/01/15 Pct Recovery = 107% Analysis Date = 08/27/15 Pct Recovery = 107% Analysis Date = 08/27/15 Pct Recovery = 107% Analysis Date = 08/23/15 Pct Recovery = 107% Analysis Date = 08/23/15 Pct Recovery = 107% Analysis Date = 08/18/15 Pct Recovery = 107% Analysis Date = 08/18/15 Pct Recovery = 107% Analysis Date = 08/13/15 Pct Recovery = 107% Analysis Date = 08/13/15 Pct Recovery = 107% Analysis Date = 08/08/15 Pct Recovery = 107% Analysis Date = 08/08/15 Pct Recovery = 107% Analysis Date = 08/03/15 Pct Recovery = 107% Analysis Date = 08/03/15 Pct Recovery = 107% Analysis Date = 07/30/15 Pct Recovery = 107% Analysis Date = 07/30/15 Pct Recovery = 107% Analysis Date = 07/25/15 Pct Recovery = 108% Analysis Date = 07/25/15 Pct Recovery = 108% Analysis Date = 07/20/15 Pct Recovery = 108% Analysis Date = 07/20/15 Pct Recovery = 108% Analysis Date = 07/15/15 Pct Recovery = 108% Analysis Date = 07/15/15 Pct Recovery = 108% Analysis Date = 07/11/15 Pct Recovery = 108% Analysis Date = 07/11/15 Pct Recovery = 108% Analysis Date = 07/06/15 Pct Recovery = 108% Analysis Date = 07/06/15 Pct Recovery = 108% Analysis Date = 07/01/15 Pct Recovery = 108% Analysis Date = 07/01/15 Pct Recovery = 108% Analysis Date = 06/26/15 Pct Recovery = 108% Analysis Date = 06/26/15 Pct Recovery = 108% Analysis Date = 06/21/15 Pct Recovery = 108% Analysis Date = 06/21/15 Pct Recovery = 108% Analysis Date = 06/17/15 Pct Recovery = 108% Analysis Date = 06/17/15 Pct Recovery = 108% Analysis Date = 06/12/15 Pct Recovery = 108% Analysis Date = 06/12/15 Pct Recovery = 108% Analysis Date = 06/07/15 Pct Recovery = 108% Analysis Date = 06/07/15 Pct Recovery = 108% Analysis Date = 06/02/15 Pct Recovery = 108% Analysis Date = 06/02/15 Pct Recovery = 108% Analysis Date = 05/29/15 Pct Recovery = 109% Analysis Date = 05/29/15 Pct Recovery = 109% Analysis Date = 05/24/15 Pct Recovery = 109% Analysis Date = 05/24/15 Pct Recovery = 109% Analysis Date = 05/19/15 Pct Recovery = 109% Analysis Date = 05/19/15 Pct Recovery = 109% Analysis Date = 05/14/15 Pct Recovery = 109% Analysis Date = 05/14/15 Pct Recovery = 109% Analysis Date = 05/10/15 Pct Recovery = 109% Analysis Date = 05/10/15 Pct Recovery = 109% Analysis Date = 05/05/15 Pct Recovery = 109% Analysis Date = 05/05/15 Pct Recovery = 109% Analysis Date = 04/30/15 Pct Recovery = 109% Analysis Date = 04/30/15 Pct Recovery = 109% Analysis Date = 04/25/15 Pct Recovery = 109% Analysis Date = 04/25/15 Pct Recovery = 109% Analysis Date = 04/20/15 Pct Recovery = 109% Analysis Date = 04/20/15 Pct Recovery = 109% Analysis Date = 04/16/15 Pct Recovery = 109% Analysis Date = 04/16/15 Pct Recovery = 109% Analysis Date = 04/11/15 Pct Recovery = 110% Analysis Date = 04/11/15 Pct Recovery = 110% Analysis Date = 04/06/15 Pct Recovery = 110% Analysis Date = 04/06/15 Pct Recovery = 110% Analysis Date = 04/01/15 Pct Recovery = 110% Analysis Date = 04/01/15 Pct Recovery = 110% Analysis Date = 03/28/15 Pct Recovery = 110% Analysis Date = 03/28/15 Pct Recovery = 110% Analysis Date = 03/23/15 Pct Recovery = 110% Analysis Date = 03/23/15 Pct Recovery = 110% Analysis Date = 03/18/15 Pct Recovery = 110% Analysis Date = 03/18/15 Pct Recovery = 110% Analysis Date = 03/13/15 Pct Recovery = 110% Analysis Date = 03/13/15 Pct Recovery = 110% Analysis Date = 03/09/15 Pct Recovery = 110% Analysis Date = 03/09/15 Pct Recovery = 110% Analysis Date = 03/04/15 Pct Recovery = 110% Analysis Date = 03/04/15 Pct Recovery = 110% Analysis Date = 02/27/15 Pct Recovery = 110% Analysis Date = 02/27/15 Pct Recovery = 110% Analysis Date = 02/22/15 Pct Recovery = 110% Analysis Date = 02/22/15 Pct Recovery = 110% Analysis Date = 02/17/15 Pct Recovery = 110% Analysis Date = 02/17/15 Pct Recovery = 110% Analysis Date = 02/13/15 Pct Recovery = 110% Analysis Date = 02/13/15 Pct Recovery = 110% Analysis Date = 02/08/15 Pct Recovery = 110% Analysis Date = 02/08/15 Pct Recovery = 110% Analysis Date = 02/03/15 Pct Recovery = 110% Analysis Date = 02/03/15 Pct Recovery = 110% Analysis Date = 01/29/15 Pct Recovery = 111% Analysis Date = 01/29/15 Pct Recovery = 111% Analysis Date = 01/25/15 Pct Recovery = 111% Analysis Date = 01/25/15 Pct Recovery = 111% Analysis Date = 01/20/15 Pct Recovery = 111% Analysis Date = 01/20/15 Pct Recovery = 111% Analysis Date = 01/15/15 Pct Recovery = 111% Analysis Date = 01/15/15 Pct Recovery = 111% Analysis Date = 01/10/15 Pct Recovery = 111% Analysis Date = 01/10/15 Pct Recovery = 111% Analysis Date = 01/06/15 Pct Recovery = 111% Analysis Date = 01/06/15 Pct Recovery = 111% Analysis Date = 01/01/15 Pct Recovery = 111% Analysis Date = 01/01/15 Pct Recovery = 111% Analysis Date = 12/27/14 Pct Recovery = 111% Analysis Date = 12/27/14 Pct Recovery = 111% Analysis Date = 12/22/14 Pct Recovery = 111% Analysis Date = 12/22/14 Pct Recovery = 111% Analysis Date = 12/17/14 Pct Recovery = 111% Analysis Date = 12/17/14 Pct Recovery = 111% Analysis Date = 12/13/14 Pct Recovery = 111% Analysis Date = 12/13/14 Pct Recovery = 111% Analysis Date = 12/08/14 Pct Recovery = 111% Analysis Date = 12/08/14 Pct Recovery = 111% Analysis Date = 12/03/14 Pct Recovery = 111% Analysis Date = 12/03/14 Pct Recovery = 111% Analysis Date = 11/28/14 Pct Recovery = 111% Analysis Date = 11/28/14 Pct Recovery = 111% Analysis Date = 11/24/14 Pct Recovery = 111% Analysis Date = 11/24/14 Pct Recovery = 111% Analysis Date = 11/19/14 Pct Recovery = 111% Analysis Date = 11/19/14 Pct Recovery = 111% Analysis Date = 11/14/14 Pct Recovery = 111% Analysis Date = 11/14/14 Pct Recovery = 111% Analysis Date = 11/09/14 Pct Recovery = 111% Analysis Date = 11/09/14 Pct Recovery = 111% Analysis Date = 11/05/14 Pct Recovery = 111% Analysis Date = 11/05/14 Pct Recovery = 111% Analysis Date = 10/31/14 Pct Recovery = 111% Analysis Date = 10/31/14 Pct Recovery = 111% Analysis Date = 10/26/14 Pct Recovery = 111% Analysis Date = 10/26/14 Pct Recovery = 111% Analysis Date = 10/21/14 Pct Recovery = 111% Analysis Date = 10/21/14 Pct Recovery = 111% Analysis Date = 10/16/14 Pct Recovery = 111% Analysis Date = 10/16/14 Pct Recovery = 111% Analysis Date = 10/12/14 Pct Recovery = 111% Analysis Date = 10/12/14 Pct Recovery = 111% Analysis Date = 10/07/14 Pct Recovery = 111% Analysis Date = 10/07/14 Pct Recovery = 111% Analysis Date = 10/02/14 Pct Recovery = 111% Analysis Date = 10/02/14 Pct Recovery = 111% Analysis Date = 09/27/14 Pct Recovery = 111% Analysis Date = 09/27/14 Pct Recovery = 111% Analysis Date = 09/23/14 Pct Recovery = 111% Analysis Date = 09/23/14 Pct Recovery = 111% Analysis Date = 09/18/14 Pct Recovery = 111% Analysis Date = 09/18/14 Pct Recovery = 111% Analysis Date = 09/13/14 Pct Recovery = 111% Analysis Date = 09/13/14 Pct Recovery = 111% Analysis Date = 09/08/14 Pct Recovery = 111% Analysis Date = 09/08/14 Pct Recovery = 111% Analysis Date = 09/04/14 Pct Recovery = 111% Analysis Date = 09/04/14 Pct Recovery = 111% Analysis Date = 08/30/14 Pct Recovery = 111% Analysis Date = 08/30/14 Pct Recovery = 111% Analysis Date = 08/25/14 Pct Recovery = 111% Analysis Date = 08/25/14 Pct Recovery = 111% Analysis Date = 08/20/14 Pct Recovery = 111% Analysis Date = 08/20/14 Pct Recovery = 111% Analysis Date = 08/15/14 Pct Recovery = 111% Analysis Date = 08/15/14 Pct Recovery = 111% Analysis Date = 08/11/14 Pct Recovery = 111% Analysis Date = 08/11/14 Pct Recovery = 111% Analysis Date = 08/06/14 Pct Recovery = 111% Analysis Date = 08/06/14 Pct Recovery = 111% Analysis Date = 08/01/14 Pct Recovery = 111% Analysis Date = 08/01/14 Pct Recovery = 111% Analysis Date = 07/27/14 Pct Recovery = 111% Analysis Date = 07/27/14 Pct Recovery = 111% Analysis Date = 07/23/14 Pct Recovery = 111% Analysis Date = 07/23/14 Pct Recovery = 111% Analysis Date = 07/18/14 Pct Recovery = 111% Analysis Date = 07/18/14 Pct Recovery = 111% Analysis Date = 07/13/14 Pct Recovery = 111% Analysis Date = 07/13/14 Pct Recovery = 111% Analysis Date = 07/08/14 Pct Recovery = 111% Analysis Date = 07/08/14 Pct Recovery = 111% Analysis Date = 07/04/14 Pct Recovery = 111% Analysis Date = 07/04/14 Pct Recovery = 111% Analysis Date = 06/29/14 Pct Recovery = 111% Analysis Date = 06/29/14 Pct Recovery = 111% Analysis Date = 06/24/14 Pct Recovery = 111% Analysis Date = 06/24/14 Pct Recovery = 111% Analysis Date = 06/19/14 Pct Recovery = 111% Analysis Date = 06/19/14 Pct Recovery = 111% Analysis Date = 06/14/14 Pct Recovery = 111% Analysis Date = 06/14/14 Pct Recovery = 111% Analysis Date = 06/10/14 Pct Recovery = 111% Analysis Date = 06/10/14 Pct Recovery = 111% Analysis Date = 06/05/14 Pct Recovery = 110% Analysis Date = 06/05/14 Pct Recovery = 110% Analysis Date = 05/31/14 Pct Recovery = 110% Analysis Date = 05/31/14 Pct Recovery = 110% Analysis Date = 05/26/14 Pct Recovery = 110% Analysis Date = 05/26/14 Pct Recovery = 110% Analysis Date = 05/22/14 Pct Recovery = 110% Analysis Date = 05/22/14 Pct Recovery = 110% Analysis Date = 05/17/14 Pct Recovery = 110% Analysis Date = 05/17/14 Pct Recovery = 110% Analysis Date = 05/12/14 Pct Recovery = 110% Analysis Date = 05/12/14 Pct Recovery = 110% Analysis Date = 05/07/14 Pct Recovery = 110% Analysis Date = 05/07/14 Pct Recovery = 110% Analysis Date = 05/03/14 Pct Recovery = 110% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
DICHLOROMETHANE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 47 114% 18% 112% 16%
Total 47 114% 18% 112% 16%

Sample Statistics
DICHLOROMETHANE

Characteristic N % % Basis
Plotted 47 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 47 .  
False Negatives 0 0% 0 out of 47
Not Spiked 26 .  
False Positives 5 19% 5 out of 26

BQS OBSP Determination:
DIETHYL ETHER
METHOD: 4440 , TESTIDCODE: 81576GCM66
Open Data Set

Analysis Date = 12/12/16 SpikeMix = Accu 216041125: 40 µl & Crescent 03FF058: 40 µl Pct Recovery = 101% Analysis Date = 07/20/16 SpikeMix = Supelco LC20141V: 40 µl & Accu 216041125: 40 µl Pct Recovery = 98% Analysis Date = 07/14/16 SpikeMix = Accu 216041125: 40 µl & NSI 041816AVOC: 40 µl Pct Recovery = 94% Analysis Date = 08/12/16 SpikeMix = ChemService 5082900: 25 µl & Phenova B20160319: 25 µl Pct Recovery = 112% Analysis Date = 06/21/16 SpikeMix = Phenova B20160319: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 113% Analysis Date = 09/08/16 SpikeMix = Supelco LC20141V: 25 µl & Accu 216041125: 25 µl Pct Recovery = 82% Analysis Date = 05/24/16 SpikeMix = Accu 216041125: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 100% Analysis Date = 04/09/15 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 88% Analysis Date = 03/19/15 SpikeMix = Spex Organics C1140417015: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 98% Analysis Date = 12/17/14 SpikeMix = Supelco LC06438: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 103% Analysis Date = 11/14/14 SpikeMix = Crescent 03DD004: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 107% Analysis Date = 08/19/14 SpikeMix = Spex Organics C1140417015: 20 µl & Accu 214031115: 20 µl Pct Recovery = 127% Analysis Date = 07/01/14 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 105% Analysis Date = 06/10/14 SpikeMix = Crescent 03DD004: 20 µl & NSI 032614: 20 µl Pct Recovery = 92% Analysis Date = 05/01/14 SpikeMix = Accu 214031115: 20 µl & NSI 032614: 20 µl Pct Recovery = 103% Analysis Date = 09/29/15 SpikeMix = Accu 215041380: 25 µl & ERA 0406-15-03: 25 µl Pct Recovery = 109% Analysis Date = 06/16/15 SpikeMix = ERA 0406-15-03: 25 µl & Supelco LC13545: 25 µl Pct Recovery = 103% Analysis Date = 07/13/15 SpikeMix = Crescent 04EE008: 25 µl & NSI 050515AVOC: 25 µl Pct Recovery = 115% Analysis Date = 11/29/16 SpikeMix = ChemService 5082900: 15 µl & Phenova B20160319: 15 µl Pct Recovery = 105% Analysis Date = 09/08/16 SpikeMix = Phenova B20160319: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 106% Analysis Date = 07/29/16 SpikeMix = Phenova B20160319: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 107% Analysis Date = 05/27/16 SpikeMix = Phenova B20160319: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 109% Analysis Date = 10/13/16 SpikeMix = Accu 216041125: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 105% Analysis Date = 08/20/16 SpikeMix = Accu 216041125: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 109% Analysis Date = 06/30/16 SpikeMix = ChemService 5082900: 15 µl & Accu 216041125: 15 µl Pct Recovery = 70% Analysis Date = 04/26/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 144% Analysis Date = 03/04/16 SpikeMix = Accu 215041380: 15 µl & ERA 0406-15-03: 15 µl Pct Recovery = 115% Analysis Date = 02/05/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 104% Analysis Date = 10/16/15 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 116% Analysis Date = 11/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 113% Analysis Date = 10/17/15 SpikeMix = Crescent 04EE008: 15 µl & NSI 050515AVOC: 15 µl Pct Recovery = 95% Analysis Date = 06/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Accu 215041380: 15 µl Pct Recovery = 100% Analysis Date = 01/13/15 SpikeMix = Accu 214031115: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 116% Analysis Date = 11/06/14 SpikeMix = Spex Organics C1140417015: 10 µl & Crescent 03DD004: 10 µl Pct Recovery = 103% Analysis Date = 10/04/14 SpikeMix = Crescent 03DD004: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 97% Analysis Date = 09/09/14 SpikeMix = Accu 214031115: 10 µl & NSI 032614: 10 µl Pct Recovery = 123% Analysis Date = 07/29/14 SpikeMix = Crescent 03DD004: 10 µl & NSI 032614: 10 µl Pct Recovery = 110% Analysis Date = 07/23/14 SpikeMix = Spex Organics C1140417015: 10 µl & Accu 214031115: 10 µl Pct Recovery = 133% Analysis Date = 06/18/14 SpikeMix = Supelco LC06438: 10 µl & Accu 214031115: 10 µl Pct Recovery = 113% Analysis Date = 05/03/14 SpikeMix = Crescent 03DD004: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 99% Analysis Date = 11/20/15 SpikeMix = Accu 215041380: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 120% Analysis Date = 07/31/15 SpikeMix = Crescent 04EE008: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 107% Analysis Date = 06/27/15 SpikeMix = ERA 0406-15-03: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 126% Analysis Date = 03/17/16 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 98% Analysis Date = 01/27/16 SpikeMix = Crescent 04EE008: 10 µl & NSI 050515AVOC: 10 µl Pct Recovery = 92% Analysis Date = 12/10/15 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 101% Analysis Date = 09/03/15 SpikeMix = NSI 050515AVOC: 10 µl & Spex Organics EN150428007: 10 µl Pct Recovery = 97% Analysis Date = 12/11/16 Pct Recovery = 100% Analysis Date = 12/07/16 Pct Recovery = 100% Analysis Date = 12/07/16 Pct Recovery = 100% Analysis Date = 12/02/16 Pct Recovery = 100% Analysis Date = 12/02/16 Pct Recovery = 100% Analysis Date = 11/27/16 Pct Recovery = 100% Analysis Date = 11/27/16 Pct Recovery = 100% Analysis Date = 11/22/16 Pct Recovery = 100% Analysis Date = 11/22/16 Pct Recovery = 100% Analysis Date = 11/18/16 Pct Recovery = 100% Analysis Date = 11/18/16 Pct Recovery = 100% Analysis Date = 11/13/16 Pct Recovery = 101% Analysis Date = 11/13/16 Pct Recovery = 101% Analysis Date = 11/08/16 Pct Recovery = 101% Analysis Date = 11/08/16 Pct Recovery = 101% Analysis Date = 11/03/16 Pct Recovery = 101% Analysis Date = 11/03/16 Pct Recovery = 101% Analysis Date = 10/29/16 Pct Recovery = 101% Analysis Date = 10/29/16 Pct Recovery = 101% Analysis Date = 10/25/16 Pct Recovery = 101% Analysis Date = 10/25/16 Pct Recovery = 101% Analysis Date = 10/20/16 Pct Recovery = 101% Analysis Date = 10/20/16 Pct Recovery = 101% Analysis Date = 10/15/16 Pct Recovery = 101% Analysis Date = 10/15/16 Pct Recovery = 101% Analysis Date = 10/10/16 Pct Recovery = 101% Analysis Date = 10/10/16 Pct Recovery = 101% Analysis Date = 10/06/16 Pct Recovery = 101% Analysis Date = 10/06/16 Pct Recovery = 101% Analysis Date = 10/01/16 Pct Recovery = 102% Analysis Date = 10/01/16 Pct Recovery = 102% Analysis Date = 09/26/16 Pct Recovery = 102% Analysis Date = 09/26/16 Pct Recovery = 102% Analysis Date = 09/21/16 Pct Recovery = 102% Analysis Date = 09/21/16 Pct Recovery = 102% Analysis Date = 09/16/16 Pct Recovery = 102% Analysis Date = 09/16/16 Pct Recovery = 102% Analysis Date = 09/12/16 Pct Recovery = 102% Analysis Date = 09/12/16 Pct Recovery = 102% Analysis Date = 09/07/16 Pct Recovery = 102% Analysis Date = 09/07/16 Pct Recovery = 102% Analysis Date = 09/02/16 Pct Recovery = 102% Analysis Date = 09/02/16 Pct Recovery = 102% Analysis Date = 08/28/16 Pct Recovery = 102% Analysis Date = 08/28/16 Pct Recovery = 102% Analysis Date = 08/24/16 Pct Recovery = 102% Analysis Date = 08/24/16 Pct Recovery = 102% Analysis Date = 08/19/16 Pct Recovery = 103% Analysis Date = 08/19/16 Pct Recovery = 103% Analysis Date = 08/14/16 Pct Recovery = 103% Analysis Date = 08/14/16 Pct Recovery = 103% Analysis Date = 08/09/16 Pct Recovery = 103% Analysis Date = 08/09/16 Pct Recovery = 103% Analysis Date = 08/04/16 Pct Recovery = 103% Analysis Date = 08/04/16 Pct Recovery = 103% Analysis Date = 07/31/16 Pct Recovery = 103% Analysis Date = 07/31/16 Pct Recovery = 103% Analysis Date = 07/26/16 Pct Recovery = 103% Analysis Date = 07/26/16 Pct Recovery = 103% Analysis Date = 07/21/16 Pct Recovery = 103% Analysis Date = 07/21/16 Pct Recovery = 103% Analysis Date = 07/16/16 Pct Recovery = 103% Analysis Date = 07/16/16 Pct Recovery = 103% Analysis Date = 07/12/16 Pct Recovery = 103% Analysis Date = 07/12/16 Pct Recovery = 103% Analysis Date = 07/07/16 Pct Recovery = 103% Analysis Date = 07/07/16 Pct Recovery = 103% Analysis Date = 07/02/16 Pct Recovery = 103% Analysis Date = 07/02/16 Pct Recovery = 103% Analysis Date = 06/27/16 Pct Recovery = 104% Analysis Date = 06/27/16 Pct Recovery = 104% Analysis Date = 06/22/16 Pct Recovery = 104% Analysis Date = 06/22/16 Pct Recovery = 104% Analysis Date = 06/18/16 Pct Recovery = 104% Analysis Date = 06/18/16 Pct Recovery = 104% Analysis Date = 06/13/16 Pct Recovery = 104% Analysis Date = 06/13/16 Pct Recovery = 104% Analysis Date = 06/08/16 Pct Recovery = 104% Analysis Date = 06/08/16 Pct Recovery = 104% Analysis Date = 06/03/16 Pct Recovery = 104% Analysis Date = 06/03/16 Pct Recovery = 104% Analysis Date = 05/30/16 Pct Recovery = 104% Analysis Date = 05/30/16 Pct Recovery = 104% Analysis Date = 05/25/16 Pct Recovery = 104% Analysis Date = 05/25/16 Pct Recovery = 104% Analysis Date = 05/20/16 Pct Recovery = 104% Analysis Date = 05/20/16 Pct Recovery = 104% Analysis Date = 05/15/16 Pct Recovery = 104% Analysis Date = 05/15/16 Pct Recovery = 104% Analysis Date = 05/10/16 Pct Recovery = 104% Analysis Date = 05/10/16 Pct Recovery = 104% Analysis Date = 05/06/16 Pct Recovery = 105% Analysis Date = 05/06/16 Pct Recovery = 105% Analysis Date = 05/01/16 Pct Recovery = 105% Analysis Date = 05/01/16 Pct Recovery = 105% Analysis Date = 04/26/16 Pct Recovery = 105% Analysis Date = 04/26/16 Pct Recovery = 105% Analysis Date = 04/21/16 Pct Recovery = 105% Analysis Date = 04/21/16 Pct Recovery = 105% Analysis Date = 04/16/16 Pct Recovery = 105% Analysis Date = 04/16/16 Pct Recovery = 105% Analysis Date = 04/12/16 Pct Recovery = 105% Analysis Date = 04/12/16 Pct Recovery = 105% Analysis Date = 04/07/16 Pct Recovery = 105% Analysis Date = 04/07/16 Pct Recovery = 105% Analysis Date = 04/02/16 Pct Recovery = 105% Analysis Date = 04/02/16 Pct Recovery = 105% Analysis Date = 03/28/16 Pct Recovery = 105% Analysis Date = 03/28/16 Pct Recovery = 105% Analysis Date = 03/24/16 Pct Recovery = 106% Analysis Date = 03/24/16 Pct Recovery = 106% Analysis Date = 03/19/16 Pct Recovery = 106% Analysis Date = 03/19/16 Pct Recovery = 106% Analysis Date = 03/14/16 Pct Recovery = 106% Analysis Date = 03/14/16 Pct Recovery = 106% Analysis Date = 03/09/16 Pct Recovery = 106% Analysis Date = 03/09/16 Pct Recovery = 106% Analysis Date = 03/04/16 Pct Recovery = 106% Analysis Date = 03/04/16 Pct Recovery = 106% Analysis Date = 02/29/16 Pct Recovery = 106% Analysis Date = 02/29/16 Pct Recovery = 106% Analysis Date = 02/24/16 Pct Recovery = 106% Analysis Date = 02/24/16 Pct Recovery = 106% Analysis Date = 02/19/16 Pct Recovery = 106% Analysis Date = 02/19/16 Pct Recovery = 106% Analysis Date = 02/14/16 Pct Recovery = 106% Analysis Date = 02/14/16 Pct Recovery = 106% Analysis Date = 02/10/16 Pct Recovery = 107% Analysis Date = 02/10/16 Pct Recovery = 107% Analysis Date = 02/05/16 Pct Recovery = 107% Analysis Date = 02/05/16 Pct Recovery = 107% Analysis Date = 01/31/16 Pct Recovery = 107% Analysis Date = 01/31/16 Pct Recovery = 107% Analysis Date = 01/26/16 Pct Recovery = 107% Analysis Date = 01/26/16 Pct Recovery = 107% Analysis Date = 01/21/16 Pct Recovery = 107% Analysis Date = 01/21/16 Pct Recovery = 107% Analysis Date = 01/17/16 Pct Recovery = 107% Analysis Date = 01/17/16 Pct Recovery = 107% Analysis Date = 01/12/16 Pct Recovery = 107% Analysis Date = 01/12/16 Pct Recovery = 107% Analysis Date = 01/07/16 Pct Recovery = 107% Analysis Date = 01/07/16 Pct Recovery = 107% Analysis Date = 01/02/16 Pct Recovery = 107% Analysis Date = 01/02/16 Pct Recovery = 107% Analysis Date = 12/29/15 Pct Recovery = 107% Analysis Date = 12/29/15 Pct Recovery = 107% Analysis Date = 12/24/15 Pct Recovery = 107% Analysis Date = 12/24/15 Pct Recovery = 107% Analysis Date = 12/19/15 Pct Recovery = 107% Analysis Date = 12/19/15 Pct Recovery = 107% Analysis Date = 12/14/15 Pct Recovery = 107% Analysis Date = 12/14/15 Pct Recovery = 107% Analysis Date = 12/09/15 Pct Recovery = 107% Analysis Date = 12/09/15 Pct Recovery = 107% Analysis Date = 12/05/15 Pct Recovery = 107% Analysis Date = 12/05/15 Pct Recovery = 107% Analysis Date = 11/30/15 Pct Recovery = 107% Analysis Date = 11/30/15 Pct Recovery = 107% Analysis Date = 11/25/15 Pct Recovery = 108% Analysis Date = 11/25/15 Pct Recovery = 108% Analysis Date = 11/20/15 Pct Recovery = 108% Analysis Date = 11/20/15 Pct Recovery = 108% Analysis Date = 11/16/15 Pct Recovery = 108% Analysis Date = 11/16/15 Pct Recovery = 108% Analysis Date = 11/11/15 Pct Recovery = 107% Analysis Date = 11/11/15 Pct Recovery = 107% Analysis Date = 11/06/15 Pct Recovery = 107% Analysis Date = 11/06/15 Pct Recovery = 107% Analysis Date = 11/01/15 Pct Recovery = 107% Analysis Date = 11/01/15 Pct Recovery = 107% Analysis Date = 10/27/15 Pct Recovery = 107% Analysis Date = 10/27/15 Pct Recovery = 107% Analysis Date = 10/23/15 Pct Recovery = 107% Analysis Date = 10/23/15 Pct Recovery = 107% Analysis Date = 10/18/15 Pct Recovery = 107% Analysis Date = 10/18/15 Pct Recovery = 107% Analysis Date = 10/13/15 Pct Recovery = 107% Analysis Date = 10/13/15 Pct Recovery = 107% Analysis Date = 10/08/15 Pct Recovery = 107% Analysis Date = 10/08/15 Pct Recovery = 107% Analysis Date = 10/04/15 Pct Recovery = 107% Analysis Date = 10/04/15 Pct Recovery = 107% Analysis Date = 09/29/15 Pct Recovery = 107% Analysis Date = 09/29/15 Pct Recovery = 107% Analysis Date = 09/24/15 Pct Recovery = 107% Analysis Date = 09/24/15 Pct Recovery = 107% Analysis Date = 09/19/15 Pct Recovery = 107% Analysis Date = 09/19/15 Pct Recovery = 107% Analysis Date = 09/14/15 Pct Recovery = 107% Analysis Date = 09/14/15 Pct Recovery = 107% Analysis Date = 09/10/15 Pct Recovery = 107% Analysis Date = 09/10/15 Pct Recovery = 107% Analysis Date = 09/05/15 Pct Recovery = 107% Analysis Date = 09/05/15 Pct Recovery = 107% Analysis Date = 08/31/15 Pct Recovery = 106% Analysis Date = 08/31/15 Pct Recovery = 106% Analysis Date = 08/26/15 Pct Recovery = 106% Analysis Date = 08/26/15 Pct Recovery = 106% Analysis Date = 08/21/15 Pct Recovery = 106% Analysis Date = 08/21/15 Pct Recovery = 106% Analysis Date = 08/17/15 Pct Recovery = 106% Analysis Date = 08/17/15 Pct Recovery = 106% Analysis Date = 08/12/15 Pct Recovery = 106% Analysis Date = 08/12/15 Pct Recovery = 106% Analysis Date = 08/07/15 Pct Recovery = 106% Analysis Date = 08/07/15 Pct Recovery = 106% Analysis Date = 08/02/15 Pct Recovery = 106% Analysis Date = 08/02/15 Pct Recovery = 106% Analysis Date = 07/29/15 Pct Recovery = 106% Analysis Date = 07/29/15 Pct Recovery = 106% Analysis Date = 07/24/15 Pct Recovery = 106% Analysis Date = 07/24/15 Pct Recovery = 106% Analysis Date = 07/19/15 Pct Recovery = 106% Analysis Date = 07/19/15 Pct Recovery = 106% Analysis Date = 07/14/15 Pct Recovery = 106% Analysis Date = 07/14/15 Pct Recovery = 106% Analysis Date = 07/09/15 Pct Recovery = 106% Analysis Date = 07/09/15 Pct Recovery = 106% Analysis Date = 07/05/15 Pct Recovery = 106% Analysis Date = 07/05/15 Pct Recovery = 106% Analysis Date = 06/30/15 Pct Recovery = 106% Analysis Date = 06/30/15 Pct Recovery = 106% Analysis Date = 06/25/15 Pct Recovery = 106% Analysis Date = 06/25/15 Pct Recovery = 106% Analysis Date = 06/20/15 Pct Recovery = 106% Analysis Date = 06/20/15 Pct Recovery = 106% Analysis Date = 06/16/15 Pct Recovery = 106% Analysis Date = 06/16/15 Pct Recovery = 106% Analysis Date = 06/11/15 Pct Recovery = 106% Analysis Date = 06/11/15 Pct Recovery = 106% Analysis Date = 06/06/15 Pct Recovery = 106% Analysis Date = 06/06/15 Pct Recovery = 106% Analysis Date = 06/01/15 Pct Recovery = 106% Analysis Date = 06/01/15 Pct Recovery = 106% Analysis Date = 05/27/15 Pct Recovery = 106% Analysis Date = 05/27/15 Pct Recovery = 106% Analysis Date = 05/23/15 Pct Recovery = 106% Analysis Date = 05/23/15 Pct Recovery = 106% Analysis Date = 05/18/15 Pct Recovery = 106% Analysis Date = 05/18/15 Pct Recovery = 106% Analysis Date = 05/13/15 Pct Recovery = 106% Analysis Date = 05/13/15 Pct Recovery = 106% Analysis Date = 05/08/15 Pct Recovery = 106% Analysis Date = 05/08/15 Pct Recovery = 106% Analysis Date = 05/04/15 Pct Recovery = 106% Analysis Date = 05/04/15 Pct Recovery = 106% Analysis Date = 04/29/15 Pct Recovery = 106% Analysis Date = 04/29/15 Pct Recovery = 106% Analysis Date = 04/24/15 Pct Recovery = 106% Analysis Date = 04/24/15 Pct Recovery = 106% Analysis Date = 04/19/15 Pct Recovery = 107% Analysis Date = 04/19/15 Pct Recovery = 107% Analysis Date = 04/14/15 Pct Recovery = 107% Analysis Date = 04/14/15 Pct Recovery = 107% Analysis Date = 04/10/15 Pct Recovery = 107% Analysis Date = 04/10/15 Pct Recovery = 107% Analysis Date = 04/05/15 Pct Recovery = 107% Analysis Date = 04/05/15 Pct Recovery = 107% Analysis Date = 03/31/15 Pct Recovery = 107% Analysis Date = 03/31/15 Pct Recovery = 107% Analysis Date = 03/26/15 Pct Recovery = 107% Analysis Date = 03/26/15 Pct Recovery = 107% Analysis Date = 03/22/15 Pct Recovery = 107% Analysis Date = 03/22/15 Pct Recovery = 107% Analysis Date = 03/17/15 Pct Recovery = 107% Analysis Date = 03/17/15 Pct Recovery = 107% Analysis Date = 03/12/15 Pct Recovery = 107% Analysis Date = 03/12/15 Pct Recovery = 107% Analysis Date = 03/07/15 Pct Recovery = 107% Analysis Date = 03/07/15 Pct Recovery = 107% Analysis Date = 03/02/15 Pct Recovery = 107% Analysis Date = 03/02/15 Pct Recovery = 107% Analysis Date = 02/26/15 Pct Recovery = 107% Analysis Date = 02/26/15 Pct Recovery = 107% Analysis Date = 02/21/15 Pct Recovery = 107% Analysis Date = 02/21/15 Pct Recovery = 107% Analysis Date = 02/16/15 Pct Recovery = 107% Analysis Date = 02/16/15 Pct Recovery = 107% Analysis Date = 02/11/15 Pct Recovery = 107% Analysis Date = 02/11/15 Pct Recovery = 107% Analysis Date = 02/07/15 Pct Recovery = 107% Analysis Date = 02/07/15 Pct Recovery = 107% Analysis Date = 02/02/15 Pct Recovery = 107% Analysis Date = 02/02/15 Pct Recovery = 107% Analysis Date = 01/28/15 Pct Recovery = 107% Analysis Date = 01/28/15 Pct Recovery = 107% Analysis Date = 01/23/15 Pct Recovery = 107% Analysis Date = 01/23/15 Pct Recovery = 107% Analysis Date = 01/18/15 Pct Recovery = 107% Analysis Date = 01/18/15 Pct Recovery = 107% Analysis Date = 01/14/15 Pct Recovery = 107% Analysis Date = 01/14/15 Pct Recovery = 107% Analysis Date = 01/09/15 Pct Recovery = 107% Analysis Date = 01/09/15 Pct Recovery = 107% Analysis Date = 01/04/15 Pct Recovery = 107% Analysis Date = 01/04/15 Pct Recovery = 107% Analysis Date = 12/30/14 Pct Recovery = 108% Analysis Date = 12/30/14 Pct Recovery = 108% Analysis Date = 12/25/14 Pct Recovery = 108% Analysis Date = 12/25/14 Pct Recovery = 108% Analysis Date = 12/21/14 Pct Recovery = 108% Analysis Date = 12/21/14 Pct Recovery = 108% Analysis Date = 12/16/14 Pct Recovery = 108% Analysis Date = 12/16/14 Pct Recovery = 108% Analysis Date = 12/11/14 Pct Recovery = 108% Analysis Date = 12/11/14 Pct Recovery = 108% Analysis Date = 12/06/14 Pct Recovery = 108% Analysis Date = 12/06/14 Pct Recovery = 108% Analysis Date = 12/02/14 Pct Recovery = 108% Analysis Date = 12/02/14 Pct Recovery = 108% Analysis Date = 11/27/14 Pct Recovery = 108% Analysis Date = 11/27/14 Pct Recovery = 108% Analysis Date = 11/22/14 Pct Recovery = 108% Analysis Date = 11/22/14 Pct Recovery = 108% Analysis Date = 11/17/14 Pct Recovery = 108% Analysis Date = 11/17/14 Pct Recovery = 108% Analysis Date = 11/12/14 Pct Recovery = 108% Analysis Date = 11/12/14 Pct Recovery = 108% Analysis Date = 11/08/14 Pct Recovery = 108% Analysis Date = 11/08/14 Pct Recovery = 108% Analysis Date = 11/03/14 Pct Recovery = 108% Analysis Date = 11/03/14 Pct Recovery = 108% Analysis Date = 10/29/14 Pct Recovery = 108% Analysis Date = 10/29/14 Pct Recovery = 108% Analysis Date = 10/24/14 Pct Recovery = 108% Analysis Date = 10/24/14 Pct Recovery = 108% Analysis Date = 10/20/14 Pct Recovery = 108% Analysis Date = 10/20/14 Pct Recovery = 108% Analysis Date = 10/15/14 Pct Recovery = 108% Analysis Date = 10/15/14 Pct Recovery = 108% Analysis Date = 10/10/14 Pct Recovery = 108% Analysis Date = 10/10/14 Pct Recovery = 108% Analysis Date = 10/05/14 Pct Recovery = 108% Analysis Date = 10/05/14 Pct Recovery = 108% Analysis Date = 09/30/14 Pct Recovery = 108% Analysis Date = 09/30/14 Pct Recovery = 108% Analysis Date = 09/26/14 Pct Recovery = 108% Analysis Date = 09/26/14 Pct Recovery = 108% Analysis Date = 09/21/14 Pct Recovery = 108% Analysis Date = 09/21/14 Pct Recovery = 108% Analysis Date = 09/16/14 Pct Recovery = 108% Analysis Date = 09/16/14 Pct Recovery = 108% Analysis Date = 09/11/14 Pct Recovery = 108% Analysis Date = 09/11/14 Pct Recovery = 108% Analysis Date = 09/07/14 Pct Recovery = 108% Analysis Date = 09/07/14 Pct Recovery = 108% Analysis Date = 09/02/14 Pct Recovery = 108% Analysis Date = 09/02/14 Pct Recovery = 108% Analysis Date = 08/28/14 Pct Recovery = 108% Analysis Date = 08/28/14 Pct Recovery = 108% Analysis Date = 08/23/14 Pct Recovery = 108% Analysis Date = 08/23/14 Pct Recovery = 108% Analysis Date = 08/18/14 Pct Recovery = 108% Analysis Date = 08/18/14 Pct Recovery = 108% Analysis Date = 08/14/14 Pct Recovery = 108% Analysis Date = 08/14/14 Pct Recovery = 108% Analysis Date = 08/09/14 Pct Recovery = 108% Analysis Date = 08/09/14 Pct Recovery = 108% Analysis Date = 08/04/14 Pct Recovery = 108% Analysis Date = 08/04/14 Pct Recovery = 108% Analysis Date = 07/30/14 Pct Recovery = 109% Analysis Date = 07/30/14 Pct Recovery = 109% Analysis Date = 07/26/14 Pct Recovery = 109% Analysis Date = 07/26/14 Pct Recovery = 109% Analysis Date = 07/21/14 Pct Recovery = 109% Analysis Date = 07/21/14 Pct Recovery = 109% Analysis Date = 07/16/14 Pct Recovery = 109% Analysis Date = 07/16/14 Pct Recovery = 109% Analysis Date = 07/11/14 Pct Recovery = 109% Analysis Date = 07/11/14 Pct Recovery = 109% Analysis Date = 07/06/14 Pct Recovery = 109% Analysis Date = 07/06/14 Pct Recovery = 109% Analysis Date = 07/02/14 Pct Recovery = 109% Analysis Date = 07/02/14 Pct Recovery = 109% Analysis Date = 06/27/14 Pct Recovery = 109% Analysis Date = 06/27/14 Pct Recovery = 109% Analysis Date = 06/22/14 Pct Recovery = 109% Analysis Date = 06/22/14 Pct Recovery = 109% Analysis Date = 06/17/14 Pct Recovery = 109% Analysis Date = 06/17/14 Pct Recovery = 109% Analysis Date = 06/13/14 Pct Recovery = 109% Analysis Date = 06/13/14 Pct Recovery = 109% Analysis Date = 06/08/14 Pct Recovery = 109% Analysis Date = 06/08/14 Pct Recovery = 109% Analysis Date = 06/03/14 Pct Recovery = 109% Analysis Date = 06/03/14 Pct Recovery = 109% Analysis Date = 05/29/14 Pct Recovery = 109% Analysis Date = 05/29/14 Pct Recovery = 109% Analysis Date = 05/24/14 Pct Recovery = 109% Analysis Date = 05/24/14 Pct Recovery = 109% Analysis Date = 05/20/14 Pct Recovery = 109% Analysis Date = 05/20/14 Pct Recovery = 109% Analysis Date = 05/15/14 Pct Recovery = 109% Analysis Date = 05/15/14 Pct Recovery = 109% Analysis Date = 05/10/14 Pct Recovery = 109% Analysis Date = 05/10/14 Pct Recovery = 109% Analysis Date = 05/05/14 Pct Recovery = 109% Analysis Date = 05/05/14 Pct Recovery = 109% Analysis Date = 05/01/14 Pct Recovery = 109% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
DIETHYL ETHER

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 47 106% 13% 105% 11%
Total 47 106% 13% 105% 11%

Sample Statistics
DIETHYL ETHER

Characteristic N % % Basis
Plotted 47 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 47 .  
False Negatives 0 0% 0 out of 47
Not Spiked 26 .  
False Positives 0 0% 0 out of 26

BQS OBSP Determination:
DIISOPROPYL ETHER
METHOD: 4440 , TESTIDCODE: 81577GCM66
Open Data Set

Analysis Date = 12/12/16 SpikeMix = Accu 216041125: 40 µl & Crescent 03FF058: 40 µl Pct Recovery = 94% Analysis Date = 07/20/16 SpikeMix = Supelco LC20141V: 40 µl & Accu 216041125: 40 µl Pct Recovery = 89% Analysis Date = 07/14/16 SpikeMix = Accu 216041125: 40 µl & NSI 041816AVOC: 40 µl Pct Recovery = 87% Analysis Date = 08/12/16 SpikeMix = ChemService 5082900: 25 µl & Phenova B20160319: 25 µl Pct Recovery = 95% Analysis Date = 06/21/16 SpikeMix = Phenova B20160319: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 120% Analysis Date = 09/08/16 SpikeMix = Supelco LC20141V: 25 µl & Accu 216041125: 25 µl Pct Recovery = 82% Analysis Date = 05/24/16 SpikeMix = Accu 216041125: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 90% Analysis Date = 03/19/15 SpikeMix = Spex Organics C1140417015: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 113% Analysis Date = 12/17/14 SpikeMix = Supelco LC06438: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 113% Analysis Date = 11/14/14 SpikeMix = Crescent 03DD004: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 89% Analysis Date = 06/10/14 SpikeMix = Crescent 03DD004: 20 µl & NSI 032614: 20 µl Pct Recovery = 91% Analysis Date = 04/09/15 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 93% Analysis Date = 08/19/14 SpikeMix = Spex Organics C1140417015: 20 µl & Accu 214031115: 20 µl Pct Recovery = 117% Analysis Date = 07/01/14 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 110% Analysis Date = 05/01/14 SpikeMix = Accu 214031115: 20 µl & NSI 032614: 20 µl Pct Recovery = 99% Analysis Date = 09/29/15 SpikeMix = Accu 215041380: 25 µl & ERA 0406-15-03: 25 µl Pct Recovery = 90% Analysis Date = 06/16/15 SpikeMix = ERA 0406-15-03: 25 µl & Supelco LC13545: 25 µl Pct Recovery = 90% Analysis Date = 07/13/15 SpikeMix = Crescent 04EE008: 25 µl & NSI 050515AVOC: 25 µl Pct Recovery = 107% Analysis Date = 11/29/16 SpikeMix = ChemService 5082900: 15 µl & Phenova B20160319: 15 µl Pct Recovery = 94% Analysis Date = 09/08/16 SpikeMix = Phenova B20160319: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 92% Analysis Date = 07/29/16 SpikeMix = Phenova B20160319: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 96% Analysis Date = 05/27/16 SpikeMix = Phenova B20160319: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 86% Analysis Date = 10/13/16 SpikeMix = Accu 216041125: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 131% Analysis Date = 08/20/16 SpikeMix = Accu 216041125: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 101% Analysis Date = 06/30/16 SpikeMix = ChemService 5082900: 15 µl & Accu 216041125: 15 µl Pct Recovery = 68% Analysis Date = 04/26/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 116% Analysis Date = 03/04/16 SpikeMix = Accu 215041380: 15 µl & ERA 0406-15-03: 15 µl Pct Recovery = 103% Analysis Date = 02/05/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 97% Analysis Date = 10/16/15 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 103% Analysis Date = 11/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 99% Analysis Date = 10/17/15 SpikeMix = Crescent 04EE008: 15 µl & NSI 050515AVOC: 15 µl Pct Recovery = 90% Analysis Date = 06/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Accu 215041380: 15 µl Pct Recovery = 90% Analysis Date = 11/06/14 SpikeMix = Spex Organics C1140417015: 10 µl & Crescent 03DD004: 10 µl Pct Recovery = 99% Analysis Date = 10/04/14 SpikeMix = Crescent 03DD004: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 88% Analysis Date = 07/29/14 SpikeMix = Crescent 03DD004: 10 µl & NSI 032614: 10 µl Pct Recovery = 93% Analysis Date = 05/03/14 SpikeMix = Crescent 03DD004: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 115% Analysis Date = 01/13/15 SpikeMix = Accu 214031115: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 122% Analysis Date = 09/09/14 SpikeMix = Accu 214031115: 10 µl & NSI 032614: 10 µl Pct Recovery = 104% Analysis Date = 07/23/14 SpikeMix = Spex Organics C1140417015: 10 µl & Accu 214031115: 10 µl Pct Recovery = 146% Analysis Date = 06/18/14 SpikeMix = Supelco LC06438: 10 µl & Accu 214031115: 10 µl Pct Recovery = 114% Analysis Date = 11/20/15 SpikeMix = Accu 215041380: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 101% Analysis Date = 07/31/15 SpikeMix = Crescent 04EE008: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 96% Analysis Date = 06/27/15 SpikeMix = ERA 0406-15-03: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 116% Analysis Date = 03/17/16 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 100% Analysis Date = 01/27/16 SpikeMix = Crescent 04EE008: 10 µl & NSI 050515AVOC: 10 µl Pct Recovery = 98% Analysis Date = 12/10/15 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 98% Analysis Date = 09/03/15 SpikeMix = NSI 050515AVOC: 10 µl & Spex Organics EN150428007: 10 µl Pct Recovery = 91% Analysis Date = 12/11/16 Pct Recovery = 97% Analysis Date = 12/07/16 Pct Recovery = 97% Analysis Date = 12/07/16 Pct Recovery = 97% Analysis Date = 12/02/16 Pct Recovery = 97% Analysis Date = 12/02/16 Pct Recovery = 97% Analysis Date = 11/27/16 Pct Recovery = 97% Analysis Date = 11/27/16 Pct Recovery = 97% Analysis Date = 11/22/16 Pct Recovery = 97% Analysis Date = 11/22/16 Pct Recovery = 97% Analysis Date = 11/18/16 Pct Recovery = 97% Analysis Date = 11/18/16 Pct Recovery = 97% Analysis Date = 11/13/16 Pct Recovery = 97% Analysis Date = 11/13/16 Pct Recovery = 97% Analysis Date = 11/08/16 Pct Recovery = 97% Analysis Date = 11/08/16 Pct Recovery = 97% Analysis Date = 11/03/16 Pct Recovery = 97% Analysis Date = 11/03/16 Pct Recovery = 97% Analysis Date = 10/29/16 Pct Recovery = 97% Analysis Date = 10/29/16 Pct Recovery = 97% Analysis Date = 10/25/16 Pct Recovery = 97% Analysis Date = 10/25/16 Pct Recovery = 97% Analysis Date = 10/20/16 Pct Recovery = 97% Analysis Date = 10/20/16 Pct Recovery = 97% Analysis Date = 10/15/16 Pct Recovery = 97% Analysis Date = 10/15/16 Pct Recovery = 97% Analysis Date = 10/10/16 Pct Recovery = 97% Analysis Date = 10/10/16 Pct Recovery = 97% Analysis Date = 10/06/16 Pct Recovery = 97% Analysis Date = 10/06/16 Pct Recovery = 97% Analysis Date = 10/01/16 Pct Recovery = 97% Analysis Date = 10/01/16 Pct Recovery = 97% Analysis Date = 09/26/16 Pct Recovery = 97% Analysis Date = 09/26/16 Pct Recovery = 97% Analysis Date = 09/21/16 Pct Recovery = 97% Analysis Date = 09/21/16 Pct Recovery = 97% Analysis Date = 09/16/16 Pct Recovery = 97% Analysis Date = 09/16/16 Pct Recovery = 97% Analysis Date = 09/12/16 Pct Recovery = 97% Analysis Date = 09/12/16 Pct Recovery = 97% Analysis Date = 09/07/16 Pct Recovery = 97% Analysis Date = 09/07/16 Pct Recovery = 97% Analysis Date = 09/02/16 Pct Recovery = 97% Analysis Date = 09/02/16 Pct Recovery = 97% Analysis Date = 08/28/16 Pct Recovery = 97% Analysis Date = 08/28/16 Pct Recovery = 97% Analysis Date = 08/24/16 Pct Recovery = 97% Analysis Date = 08/24/16 Pct Recovery = 97% Analysis Date = 08/19/16 Pct Recovery = 97% Analysis Date = 08/19/16 Pct Recovery = 97% Analysis Date = 08/14/16 Pct Recovery = 97% Analysis Date = 08/14/16 Pct Recovery = 97% Analysis Date = 08/09/16 Pct Recovery = 97% Analysis Date = 08/09/16 Pct Recovery = 97% Analysis Date = 08/04/16 Pct Recovery = 97% Analysis Date = 08/04/16 Pct Recovery = 97% Analysis Date = 07/31/16 Pct Recovery = 97% Analysis Date = 07/31/16 Pct Recovery = 97% Analysis Date = 07/26/16 Pct Recovery = 97% Analysis Date = 07/26/16 Pct Recovery = 97% Analysis Date = 07/21/16 Pct Recovery = 97% Analysis Date = 07/21/16 Pct Recovery = 97% Analysis Date = 07/16/16 Pct Recovery = 97% Analysis Date = 07/16/16 Pct Recovery = 97% Analysis Date = 07/12/16 Pct Recovery = 97% Analysis Date = 07/12/16 Pct Recovery = 97% Analysis Date = 07/07/16 Pct Recovery = 97% Analysis Date = 07/07/16 Pct Recovery = 97% Analysis Date = 07/02/16 Pct Recovery = 97% Analysis Date = 07/02/16 Pct Recovery = 97% Analysis Date = 06/27/16 Pct Recovery = 97% Analysis Date = 06/27/16 Pct Recovery = 97% Analysis Date = 06/22/16 Pct Recovery = 97% Analysis Date = 06/22/16 Pct Recovery = 97% Analysis Date = 06/18/16 Pct Recovery = 97% Analysis Date = 06/18/16 Pct Recovery = 97% Analysis Date = 06/13/16 Pct Recovery = 97% Analysis Date = 06/13/16 Pct Recovery = 97% Analysis Date = 06/08/16 Pct Recovery = 97% Analysis Date = 06/08/16 Pct Recovery = 97% Analysis Date = 06/03/16 Pct Recovery = 97% Analysis Date = 06/03/16 Pct Recovery = 97% Analysis Date = 05/30/16 Pct Recovery = 97% Analysis Date = 05/30/16 Pct Recovery = 97% Analysis Date = 05/25/16 Pct Recovery = 97% Analysis Date = 05/25/16 Pct Recovery = 97% Analysis Date = 05/20/16 Pct Recovery = 97% Analysis Date = 05/20/16 Pct Recovery = 97% Analysis Date = 05/15/16 Pct Recovery = 97% Analysis Date = 05/15/16 Pct Recovery = 97% Analysis Date = 05/10/16 Pct Recovery = 97% Analysis Date = 05/10/16 Pct Recovery = 97% Analysis Date = 05/06/16 Pct Recovery = 97% Analysis Date = 05/06/16 Pct Recovery = 97% Analysis Date = 05/01/16 Pct Recovery = 97% Analysis Date = 05/01/16 Pct Recovery = 97% Analysis Date = 04/26/16 Pct Recovery = 97% Analysis Date = 04/26/16 Pct Recovery = 97% Analysis Date = 04/21/16 Pct Recovery = 97% Analysis Date = 04/21/16 Pct Recovery = 97% Analysis Date = 04/16/16 Pct Recovery = 97% Analysis Date = 04/16/16 Pct Recovery = 97% Analysis Date = 04/12/16 Pct Recovery = 97% Analysis Date = 04/12/16 Pct Recovery = 97% Analysis Date = 04/07/16 Pct Recovery = 97% Analysis Date = 04/07/16 Pct Recovery = 97% Analysis Date = 04/02/16 Pct Recovery = 97% Analysis Date = 04/02/16 Pct Recovery = 97% Analysis Date = 03/28/16 Pct Recovery = 97% Analysis Date = 03/28/16 Pct Recovery = 97% Analysis Date = 03/24/16 Pct Recovery = 97% Analysis Date = 03/24/16 Pct Recovery = 97% Analysis Date = 03/19/16 Pct Recovery = 97% Analysis Date = 03/19/16 Pct Recovery = 97% Analysis Date = 03/14/16 Pct Recovery = 97% Analysis Date = 03/14/16 Pct Recovery = 97% Analysis Date = 03/09/16 Pct Recovery = 97% Analysis Date = 03/09/16 Pct Recovery = 97% Analysis Date = 03/04/16 Pct Recovery = 97% Analysis Date = 03/04/16 Pct Recovery = 97% Analysis Date = 02/29/16 Pct Recovery = 97% Analysis Date = 02/29/16 Pct Recovery = 97% Analysis Date = 02/24/16 Pct Recovery = 97% Analysis Date = 02/24/16 Pct Recovery = 97% Analysis Date = 02/19/16 Pct Recovery = 97% Analysis Date = 02/19/16 Pct Recovery = 97% Analysis Date = 02/14/16 Pct Recovery = 97% Analysis Date = 02/14/16 Pct Recovery = 97% Analysis Date = 02/10/16 Pct Recovery = 97% Analysis Date = 02/10/16 Pct Recovery = 97% Analysis Date = 02/05/16 Pct Recovery = 97% Analysis Date = 02/05/16 Pct Recovery = 97% Analysis Date = 01/31/16 Pct Recovery = 97% Analysis Date = 01/31/16 Pct Recovery = 97% Analysis Date = 01/26/16 Pct Recovery = 97% Analysis Date = 01/26/16 Pct Recovery = 97% Analysis Date = 01/21/16 Pct Recovery = 97% Analysis Date = 01/21/16 Pct Recovery = 97% Analysis Date = 01/17/16 Pct Recovery = 97% Analysis Date = 01/17/16 Pct Recovery = 97% Analysis Date = 01/12/16 Pct Recovery = 97% Analysis Date = 01/12/16 Pct Recovery = 97% Analysis Date = 01/07/16 Pct Recovery = 98% Analysis Date = 01/07/16 Pct Recovery = 98% Analysis Date = 01/02/16 Pct Recovery = 98% Analysis Date = 01/02/16 Pct Recovery = 98% Analysis Date = 12/29/15 Pct Recovery = 98% Analysis Date = 12/29/15 Pct Recovery = 98% Analysis Date = 12/24/15 Pct Recovery = 98% Analysis Date = 12/24/15 Pct Recovery = 98% Analysis Date = 12/19/15 Pct Recovery = 98% Analysis Date = 12/19/15 Pct Recovery = 98% Analysis Date = 12/14/15 Pct Recovery = 98% Analysis Date = 12/14/15 Pct Recovery = 98% Analysis Date = 12/09/15 Pct Recovery = 98% Analysis Date = 12/09/15 Pct Recovery = 98% Analysis Date = 12/05/15 Pct Recovery = 98% Analysis Date = 12/05/15 Pct Recovery = 98% Analysis Date = 11/30/15 Pct Recovery = 98% Analysis Date = 11/30/15 Pct Recovery = 98% Analysis Date = 11/25/15 Pct Recovery = 98% Analysis Date = 11/25/15 Pct Recovery = 98% Analysis Date = 11/20/15 Pct Recovery = 98% Analysis Date = 11/20/15 Pct Recovery = 98% Analysis Date = 11/16/15 Pct Recovery = 98% Analysis Date = 11/16/15 Pct Recovery = 98% Analysis Date = 11/11/15 Pct Recovery = 98% Analysis Date = 11/11/15 Pct Recovery = 98% Analysis Date = 11/06/15 Pct Recovery = 98% Analysis Date = 11/06/15 Pct Recovery = 98% Analysis Date = 11/01/15 Pct Recovery = 98% Analysis Date = 11/01/15 Pct Recovery = 98% Analysis Date = 10/27/15 Pct Recovery = 98% Analysis Date = 10/27/15 Pct Recovery = 98% Analysis Date = 10/23/15 Pct Recovery = 98% Analysis Date = 10/23/15 Pct Recovery = 98% Analysis Date = 10/18/15 Pct Recovery = 98% Analysis Date = 10/18/15 Pct Recovery = 98% Analysis Date = 10/13/15 Pct Recovery = 98% Analysis Date = 10/13/15 Pct Recovery = 98% Analysis Date = 10/08/15 Pct Recovery = 98% Analysis Date = 10/08/15 Pct Recovery = 98% Analysis Date = 10/04/15 Pct Recovery = 98% Analysis Date = 10/04/15 Pct Recovery = 98% Analysis Date = 09/29/15 Pct Recovery = 99% Analysis Date = 09/29/15 Pct Recovery = 99% Analysis Date = 09/24/15 Pct Recovery = 99% Analysis Date = 09/24/15 Pct Recovery = 99% Analysis Date = 09/19/15 Pct Recovery = 99% Analysis Date = 09/19/15 Pct Recovery = 99% Analysis Date = 09/14/15 Pct Recovery = 99% Analysis Date = 09/14/15 Pct Recovery = 99% Analysis Date = 09/10/15 Pct Recovery = 99% Analysis Date = 09/10/15 Pct Recovery = 99% Analysis Date = 09/05/15 Pct Recovery = 99% Analysis Date = 09/05/15 Pct Recovery = 99% Analysis Date = 08/31/15 Pct Recovery = 99% Analysis Date = 08/31/15 Pct Recovery = 99% Analysis Date = 08/26/15 Pct Recovery = 99% Analysis Date = 08/26/15 Pct Recovery = 99% Analysis Date = 08/21/15 Pct Recovery = 99% Analysis Date = 08/21/15 Pct Recovery = 99% Analysis Date = 08/17/15 Pct Recovery = 99% Analysis Date = 08/17/15 Pct Recovery = 99% Analysis Date = 08/12/15 Pct Recovery = 99% Analysis Date = 08/12/15 Pct Recovery = 99% Analysis Date = 08/07/15 Pct Recovery = 100% Analysis Date = 08/07/15 Pct Recovery = 100% Analysis Date = 08/02/15 Pct Recovery = 100% Analysis Date = 08/02/15 Pct Recovery = 100% Analysis Date = 07/29/15 Pct Recovery = 100% Analysis Date = 07/29/15 Pct Recovery = 100% Analysis Date = 07/24/15 Pct Recovery = 100% Analysis Date = 07/24/15 Pct Recovery = 100% Analysis Date = 07/19/15 Pct Recovery = 100% Analysis Date = 07/19/15 Pct Recovery = 100% Analysis Date = 07/14/15 Pct Recovery = 100% Analysis Date = 07/14/15 Pct Recovery = 100% Analysis Date = 07/09/15 Pct Recovery = 100% Analysis Date = 07/09/15 Pct Recovery = 100% Analysis Date = 07/05/15 Pct Recovery = 100% Analysis Date = 07/05/15 Pct Recovery = 100% Analysis Date = 06/30/15 Pct Recovery = 100% Analysis Date = 06/30/15 Pct Recovery = 100% Analysis Date = 06/25/15 Pct Recovery = 100% Analysis Date = 06/25/15 Pct Recovery = 100% Analysis Date = 06/20/15 Pct Recovery = 100% Analysis Date = 06/20/15 Pct Recovery = 100% Analysis Date = 06/16/15 Pct Recovery = 100% Analysis Date = 06/16/15 Pct Recovery = 100% Analysis Date = 06/11/15 Pct Recovery = 100% Analysis Date = 06/11/15 Pct Recovery = 100% Analysis Date = 06/06/15 Pct Recovery = 101% Analysis Date = 06/06/15 Pct Recovery = 101% Analysis Date = 06/01/15 Pct Recovery = 101% Analysis Date = 06/01/15 Pct Recovery = 101% Analysis Date = 05/27/15 Pct Recovery = 101% Analysis Date = 05/27/15 Pct Recovery = 101% Analysis Date = 05/23/15 Pct Recovery = 101% Analysis Date = 05/23/15 Pct Recovery = 101% Analysis Date = 05/18/15 Pct Recovery = 101% Analysis Date = 05/18/15 Pct Recovery = 101% Analysis Date = 05/13/15 Pct Recovery = 101% Analysis Date = 05/13/15 Pct Recovery = 101% Analysis Date = 05/08/15 Pct Recovery = 101% Analysis Date = 05/08/15 Pct Recovery = 101% Analysis Date = 05/04/15 Pct Recovery = 101% Analysis Date = 05/04/15 Pct Recovery = 101% Analysis Date = 04/29/15 Pct Recovery = 101% Analysis Date = 04/29/15 Pct Recovery = 101% Analysis Date = 04/24/15 Pct Recovery = 101% Analysis Date = 04/24/15 Pct Recovery = 101% Analysis Date = 04/19/15 Pct Recovery = 101% Analysis Date = 04/19/15 Pct Recovery = 101% Analysis Date = 04/14/15 Pct Recovery = 102% Analysis Date = 04/14/15 Pct Recovery = 102% Analysis Date = 04/10/15 Pct Recovery = 102% Analysis Date = 04/10/15 Pct Recovery = 102% Analysis Date = 04/05/15 Pct Recovery = 102% Analysis Date = 04/05/15 Pct Recovery = 102% Analysis Date = 03/31/15 Pct Recovery = 102% Analysis Date = 03/31/15 Pct Recovery = 102% Analysis Date = 03/26/15 Pct Recovery = 102% Analysis Date = 03/26/15 Pct Recovery = 102% Analysis Date = 03/22/15 Pct Recovery = 102% Analysis Date = 03/22/15 Pct Recovery = 102% Analysis Date = 03/17/15 Pct Recovery = 102% Analysis Date = 03/17/15 Pct Recovery = 102% Analysis Date = 03/12/15 Pct Recovery = 102% Analysis Date = 03/12/15 Pct Recovery = 102% Analysis Date = 03/07/15 Pct Recovery = 102% Analysis Date = 03/07/15 Pct Recovery = 102% Analysis Date = 03/02/15 Pct Recovery = 102% Analysis Date = 03/02/15 Pct Recovery = 102% Analysis Date = 02/26/15 Pct Recovery = 103% Analysis Date = 02/26/15 Pct Recovery = 103% Analysis Date = 02/21/15 Pct Recovery = 103% Analysis Date = 02/21/15 Pct Recovery = 103% Analysis Date = 02/16/15 Pct Recovery = 103% Analysis Date = 02/16/15 Pct Recovery = 103% Analysis Date = 02/11/15 Pct Recovery = 103% Analysis Date = 02/11/15 Pct Recovery = 103% Analysis Date = 02/07/15 Pct Recovery = 103% Analysis Date = 02/07/15 Pct Recovery = 103% Analysis Date = 02/02/15 Pct Recovery = 103% Analysis Date = 02/02/15 Pct Recovery = 103% Analysis Date = 01/28/15 Pct Recovery = 103% Analysis Date = 01/28/15 Pct Recovery = 103% Analysis Date = 01/23/15 Pct Recovery = 103% Analysis Date = 01/23/15 Pct Recovery = 103% Analysis Date = 01/18/15 Pct Recovery = 104% Analysis Date = 01/18/15 Pct Recovery = 104% Analysis Date = 01/14/15 Pct Recovery = 104% Analysis Date = 01/14/15 Pct Recovery = 104% Analysis Date = 01/09/15 Pct Recovery = 104% Analysis Date = 01/09/15 Pct Recovery = 104% Analysis Date = 01/04/15 Pct Recovery = 104% Analysis Date = 01/04/15 Pct Recovery = 104% Analysis Date = 12/30/14 Pct Recovery = 104% Analysis Date = 12/30/14 Pct Recovery = 104% Analysis Date = 12/25/14 Pct Recovery = 104% Analysis Date = 12/25/14 Pct Recovery = 104% Analysis Date = 12/21/14 Pct Recovery = 104% Analysis Date = 12/21/14 Pct Recovery = 104% Analysis Date = 12/16/14 Pct Recovery = 104% Analysis Date = 12/16/14 Pct Recovery = 104% Analysis Date = 12/11/14 Pct Recovery = 105% Analysis Date = 12/11/14 Pct Recovery = 105% Analysis Date = 12/06/14 Pct Recovery = 105% Analysis Date = 12/06/14 Pct Recovery = 105% Analysis Date = 12/02/14 Pct Recovery = 105% Analysis Date = 12/02/14 Pct Recovery = 105% Analysis Date = 11/27/14 Pct Recovery = 105% Analysis Date = 11/27/14 Pct Recovery = 105% Analysis Date = 11/22/14 Pct Recovery = 105% Analysis Date = 11/22/14 Pct Recovery = 105% Analysis Date = 11/17/14 Pct Recovery = 105% Analysis Date = 11/17/14 Pct Recovery = 105% Analysis Date = 11/12/14 Pct Recovery = 105% Analysis Date = 11/12/14 Pct Recovery = 105% Analysis Date = 11/08/14 Pct Recovery = 105% Analysis Date = 11/08/14 Pct Recovery = 105% Analysis Date = 11/03/14 Pct Recovery = 105% Analysis Date = 11/03/14 Pct Recovery = 105% Analysis Date = 10/29/14 Pct Recovery = 106% Analysis Date = 10/29/14 Pct Recovery = 106% Analysis Date = 10/24/14 Pct Recovery = 106% Analysis Date = 10/24/14 Pct Recovery = 106% Analysis Date = 10/20/14 Pct Recovery = 106% Analysis Date = 10/20/14 Pct Recovery = 106% Analysis Date = 10/15/14 Pct Recovery = 106% Analysis Date = 10/15/14 Pct Recovery = 106% Analysis Date = 10/10/14 Pct Recovery = 106% Analysis Date = 10/10/14 Pct Recovery = 106% Analysis Date = 10/05/14 Pct Recovery = 106% Analysis Date = 10/05/14 Pct Recovery = 106% Analysis Date = 09/30/14 Pct Recovery = 106% Analysis Date = 09/30/14 Pct Recovery = 106% Analysis Date = 09/26/14 Pct Recovery = 106% Analysis Date = 09/26/14 Pct Recovery = 106% Analysis Date = 09/21/14 Pct Recovery = 106% Analysis Date = 09/21/14 Pct Recovery = 106% Analysis Date = 09/16/14 Pct Recovery = 106% Analysis Date = 09/16/14 Pct Recovery = 106% Analysis Date = 09/11/14 Pct Recovery = 106% Analysis Date = 09/11/14 Pct Recovery = 106% Analysis Date = 09/07/14 Pct Recovery = 107% Analysis Date = 09/07/14 Pct Recovery = 107% Analysis Date = 09/02/14 Pct Recovery = 107% Analysis Date = 09/02/14 Pct Recovery = 107% Analysis Date = 08/28/14 Pct Recovery = 107% Analysis Date = 08/28/14 Pct Recovery = 107% Analysis Date = 08/23/14 Pct Recovery = 107% Analysis Date = 08/23/14 Pct Recovery = 107% Analysis Date = 08/18/14 Pct Recovery = 107% Analysis Date = 08/18/14 Pct Recovery = 107% Analysis Date = 08/14/14 Pct Recovery = 107% Analysis Date = 08/14/14 Pct Recovery = 107% Analysis Date = 08/09/14 Pct Recovery = 107% Analysis Date = 08/09/14 Pct Recovery = 107% Analysis Date = 08/04/14 Pct Recovery = 107% Analysis Date = 08/04/14 Pct Recovery = 107% Analysis Date = 07/30/14 Pct Recovery = 107% Analysis Date = 07/30/14 Pct Recovery = 107% Analysis Date = 07/26/14 Pct Recovery = 107% Analysis Date = 07/26/14 Pct Recovery = 107% Analysis Date = 07/21/14 Pct Recovery = 107% Analysis Date = 07/21/14 Pct Recovery = 107% Analysis Date = 07/16/14 Pct Recovery = 108% Analysis Date = 07/16/14 Pct Recovery = 108% Analysis Date = 07/11/14 Pct Recovery = 108% Analysis Date = 07/11/14 Pct Recovery = 108% Analysis Date = 07/06/14 Pct Recovery = 108% Analysis Date = 07/06/14 Pct Recovery = 108% Analysis Date = 07/02/14 Pct Recovery = 108% Analysis Date = 07/02/14 Pct Recovery = 108% Analysis Date = 06/27/14 Pct Recovery = 108% Analysis Date = 06/27/14 Pct Recovery = 108% Analysis Date = 06/22/14 Pct Recovery = 108% Analysis Date = 06/22/14 Pct Recovery = 108% Analysis Date = 06/17/14 Pct Recovery = 108% Analysis Date = 06/17/14 Pct Recovery = 108% Analysis Date = 06/13/14 Pct Recovery = 108% Analysis Date = 06/13/14 Pct Recovery = 108% Analysis Date = 06/08/14 Pct Recovery = 108% Analysis Date = 06/08/14 Pct Recovery = 108% Analysis Date = 06/03/14 Pct Recovery = 108% Analysis Date = 06/03/14 Pct Recovery = 108% Analysis Date = 05/29/14 Pct Recovery = 108% Analysis Date = 05/29/14 Pct Recovery = 108% Analysis Date = 05/24/14 Pct Recovery = 109% Analysis Date = 05/24/14 Pct Recovery = 109% Analysis Date = 05/20/14 Pct Recovery = 109% Analysis Date = 05/20/14 Pct Recovery = 109% Analysis Date = 05/15/14 Pct Recovery = 109% Analysis Date = 05/15/14 Pct Recovery = 109% Analysis Date = 05/10/14 Pct Recovery = 109% Analysis Date = 05/10/14 Pct Recovery = 109% Analysis Date = 05/05/14 Pct Recovery = 109% Analysis Date = 05/05/14 Pct Recovery = 109% Analysis Date = 05/01/14 Pct Recovery = 109% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
DIISOPROPYL ETHER

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 47 100% 14% 98% 14%
Total 47 100% 14% 98% 14%

Sample Statistics
DIISOPROPYL ETHER

Characteristic N % % Basis
Plotted 47 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 47 .  
False Negatives 0 0% 0 out of 47
Not Spiked 26 .  
False Positives 0 0% 0 out of 26

BQS OBSP Determination:
ETHYLBENZENE
METHOD: 4440 , TESTIDCODE: 34371GCM66
Open Data Set

Analysis Date = 12/12/16 SpikeMix = Accu 216041125: 40 µl & Crescent 03FF058: 40 µl Pct Recovery = 96% Analysis Date = 07/20/16 SpikeMix = Supelco LC20141V: 40 µl & Accu 216041125: 40 µl Pct Recovery = 93% Analysis Date = 07/14/16 SpikeMix = Accu 216041125: 40 µl & NSI 041816AVOC: 40 µl Pct Recovery = 80% Analysis Date = 09/08/16 SpikeMix = Supelco LC20141V: 25 µl & Accu 216041125: 25 µl Pct Recovery = 77% Analysis Date = 05/24/16 SpikeMix = Accu 216041125: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 86% Analysis Date = 08/12/16 SpikeMix = ChemService 5082900: 25 µl & Phenova B20160319: 25 µl Pct Recovery = 88% Analysis Date = 06/21/16 SpikeMix = Phenova B20160319: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 95% Analysis Date = 04/09/15 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 94% Analysis Date = 03/06/15 SpikeMix = ERA 0227-14-06.1A: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 92% Analysis Date = 11/14/14 SpikeMix = Crescent 03DD004: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 85% Analysis Date = 08/16/14 SpikeMix = ERA 0227-14-06.1A: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 98% Analysis Date = 07/01/14 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 93% Analysis Date = 11/22/14 SpikeMix = NSI 032614: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 84% Analysis Date = 06/10/14 SpikeMix = Crescent 03DD004: 20 µl & NSI 032614: 20 µl Pct Recovery = 76% Analysis Date = 06/10/14 SpikeMix = NSI 032614: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 87% Analysis Date = 05/01/14 SpikeMix = Accu 214031115: 20 µl & NSI 032614: 20 µl Pct Recovery = 76% Analysis Date = 09/29/15 SpikeMix = Accu 215041380: 25 µl & ERA 0406-15-03: 25 µl Pct Recovery = 92% Analysis Date = 06/16/15 SpikeMix = ERA 0406-15-03: 25 µl & Supelco LC13545: 25 µl Pct Recovery = 87% Analysis Date = 07/13/15 SpikeMix = Crescent 04EE008: 25 µl & NSI 050515AVOC: 25 µl Pct Recovery = 92% Analysis Date = 10/13/16 SpikeMix = Accu 216041125: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 94% Analysis Date = 08/20/16 SpikeMix = Accu 216041125: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 95% Analysis Date = 06/30/16 SpikeMix = ChemService 5082900: 15 µl & Accu 216041125: 15 µl Pct Recovery = 65% Analysis Date = 11/29/16 SpikeMix = ChemService 5082900: 15 µl & Phenova B20160319: 15 µl Pct Recovery = 89% Analysis Date = 09/08/16 SpikeMix = Phenova B20160319: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 85% Analysis Date = 07/29/16 SpikeMix = Phenova B20160319: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 86% Analysis Date = 05/27/16 SpikeMix = Phenova B20160319: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 91% Analysis Date = 04/26/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 85% Analysis Date = 03/04/16 SpikeMix = Accu 215041380: 15 µl & ERA 0406-15-03: 15 µl Pct Recovery = 88% Analysis Date = 02/05/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 93% Analysis Date = 10/16/15 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 92% Analysis Date = 11/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 86% Analysis Date = 10/17/15 SpikeMix = Crescent 04EE008: 15 µl & NSI 050515AVOC: 15 µl Pct Recovery = 89% Analysis Date = 06/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Accu 215041380: 15 µl Pct Recovery = 99% Analysis Date = 01/13/15 SpikeMix = Accu 214031115: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 98% Analysis Date = 10/21/14 SpikeMix = ERA 0227-14-06.1A: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 95% Analysis Date = 10/04/14 SpikeMix = Crescent 03DD004: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 89% Analysis Date = 07/11/14 SpikeMix = Spex Organics C1140417015: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 97% Analysis Date = 09/09/14 SpikeMix = Accu 214031115: 10 µl & NSI 032614: 10 µl Pct Recovery = 115% Analysis Date = 09/09/14 SpikeMix = NSI 032614: 10 µl & Spex Organics C1140417015: 10 µl Pct Recovery = 115% Analysis Date = 07/29/14 SpikeMix = Crescent 03DD004: 10 µl & NSI 032614: 10 µl Pct Recovery = 94% Analysis Date = 05/30/14 SpikeMix = NSI 032614: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 86% Analysis Date = 11/20/15 SpikeMix = Accu 215041380: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 103% Analysis Date = 07/31/15 SpikeMix = Crescent 04EE008: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 88% Analysis Date = 06/27/15 SpikeMix = ERA 0406-15-03: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 108% Analysis Date = 03/17/16 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 85% Analysis Date = 01/27/16 SpikeMix = Crescent 04EE008: 10 µl & NSI 050515AVOC: 10 µl Pct Recovery = 104% Analysis Date = 12/10/15 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 100% Analysis Date = 09/03/15 SpikeMix = NSI 050515AVOC: 10 µl & Spex Organics EN150428007: 10 µl Pct Recovery = 91% Analysis Date = 12/11/16 Pct Recovery = 87% Analysis Date = 12/07/16 Pct Recovery = 87% Analysis Date = 12/07/16 Pct Recovery = 87% Analysis Date = 12/02/16 Pct Recovery = 87% Analysis Date = 12/02/16 Pct Recovery = 87% Analysis Date = 11/27/16 Pct Recovery = 87% Analysis Date = 11/27/16 Pct Recovery = 87% Analysis Date = 11/22/16 Pct Recovery = 87% Analysis Date = 11/22/16 Pct Recovery = 87% Analysis Date = 11/18/16 Pct Recovery = 87% Analysis Date = 11/18/16 Pct Recovery = 87% Analysis Date = 11/13/16 Pct Recovery = 87% Analysis Date = 11/13/16 Pct Recovery = 87% Analysis Date = 11/08/16 Pct Recovery = 87% Analysis Date = 11/08/16 Pct Recovery = 87% Analysis Date = 11/03/16 Pct Recovery = 87% Analysis Date = 11/03/16 Pct Recovery = 87% Analysis Date = 10/29/16 Pct Recovery = 87% Analysis Date = 10/29/16 Pct Recovery = 87% Analysis Date = 10/25/16 Pct Recovery = 87% Analysis Date = 10/25/16 Pct Recovery = 87% Analysis Date = 10/20/16 Pct Recovery = 87% Analysis Date = 10/20/16 Pct Recovery = 87% Analysis Date = 10/15/16 Pct Recovery = 87% Analysis Date = 10/15/16 Pct Recovery = 87% Analysis Date = 10/10/16 Pct Recovery = 87% Analysis Date = 10/10/16 Pct Recovery = 87% Analysis Date = 10/06/16 Pct Recovery = 87% Analysis Date = 10/06/16 Pct Recovery = 87% Analysis Date = 10/01/16 Pct Recovery = 87% Analysis Date = 10/01/16 Pct Recovery = 87% Analysis Date = 09/26/16 Pct Recovery = 87% Analysis Date = 09/26/16 Pct Recovery = 87% Analysis Date = 09/21/16 Pct Recovery = 87% Analysis Date = 09/21/16 Pct Recovery = 87% Analysis Date = 09/16/16 Pct Recovery = 87% Analysis Date = 09/16/16 Pct Recovery = 87% Analysis Date = 09/12/16 Pct Recovery = 87% Analysis Date = 09/12/16 Pct Recovery = 87% Analysis Date = 09/07/16 Pct Recovery = 87% Analysis Date = 09/07/16 Pct Recovery = 87% Analysis Date = 09/02/16 Pct Recovery = 88% Analysis Date = 09/02/16 Pct Recovery = 88% Analysis Date = 08/28/16 Pct Recovery = 88% Analysis Date = 08/28/16 Pct Recovery = 88% Analysis Date = 08/24/16 Pct Recovery = 88% Analysis Date = 08/24/16 Pct Recovery = 88% Analysis Date = 08/19/16 Pct Recovery = 88% Analysis Date = 08/19/16 Pct Recovery = 88% Analysis Date = 08/14/16 Pct Recovery = 88% Analysis Date = 08/14/16 Pct Recovery = 88% Analysis Date = 08/09/16 Pct Recovery = 88% Analysis Date = 08/09/16 Pct Recovery = 88% Analysis Date = 08/04/16 Pct Recovery = 88% Analysis Date = 08/04/16 Pct Recovery = 88% Analysis Date = 07/31/16 Pct Recovery = 88% Analysis Date = 07/31/16 Pct Recovery = 88% Analysis Date = 07/26/16 Pct Recovery = 88% Analysis Date = 07/26/16 Pct Recovery = 88% Analysis Date = 07/21/16 Pct Recovery = 88% Analysis Date = 07/21/16 Pct Recovery = 88% Analysis Date = 07/16/16 Pct Recovery = 88% Analysis Date = 07/16/16 Pct Recovery = 88% Analysis Date = 07/12/16 Pct Recovery = 88% Analysis Date = 07/12/16 Pct Recovery = 88% Analysis Date = 07/07/16 Pct Recovery = 88% Analysis Date = 07/07/16 Pct Recovery = 88% Analysis Date = 07/02/16 Pct Recovery = 88% Analysis Date = 07/02/16 Pct Recovery = 88% Analysis Date = 06/27/16 Pct Recovery = 88% Analysis Date = 06/27/16 Pct Recovery = 88% Analysis Date = 06/22/16 Pct Recovery = 88% Analysis Date = 06/22/16 Pct Recovery = 88% Analysis Date = 06/18/16 Pct Recovery = 88% Analysis Date = 06/18/16 Pct Recovery = 88% Analysis Date = 06/13/16 Pct Recovery = 88% Analysis Date = 06/13/16 Pct Recovery = 88% Analysis Date = 06/08/16 Pct Recovery = 88% Analysis Date = 06/08/16 Pct Recovery = 88% Analysis Date = 06/03/16 Pct Recovery = 89% Analysis Date = 06/03/16 Pct Recovery = 89% Analysis Date = 05/30/16 Pct Recovery = 89% Analysis Date = 05/30/16 Pct Recovery = 89% Analysis Date = 05/25/16 Pct Recovery = 89% Analysis Date = 05/25/16 Pct Recovery = 89% Analysis Date = 05/20/16 Pct Recovery = 89% Analysis Date = 05/20/16 Pct Recovery = 89% Analysis Date = 05/15/16 Pct Recovery = 89% Analysis Date = 05/15/16 Pct Recovery = 89% Analysis Date = 05/10/16 Pct Recovery = 89% Analysis Date = 05/10/16 Pct Recovery = 89% Analysis Date = 05/06/16 Pct Recovery = 89% Analysis Date = 05/06/16 Pct Recovery = 89% Analysis Date = 05/01/16 Pct Recovery = 89% Analysis Date = 05/01/16 Pct Recovery = 89% Analysis Date = 04/26/16 Pct Recovery = 89% Analysis Date = 04/26/16 Pct Recovery = 89% Analysis Date = 04/21/16 Pct Recovery = 89% Analysis Date = 04/21/16 Pct Recovery = 89% Analysis Date = 04/16/16 Pct Recovery = 89% Analysis Date = 04/16/16 Pct Recovery = 89% Analysis Date = 04/12/16 Pct Recovery = 90% Analysis Date = 04/12/16 Pct Recovery = 90% Analysis Date = 04/07/16 Pct Recovery = 90% Analysis Date = 04/07/16 Pct Recovery = 90% Analysis Date = 04/02/16 Pct Recovery = 90% Analysis Date = 04/02/16 Pct Recovery = 90% Analysis Date = 03/28/16 Pct Recovery = 90% Analysis Date = 03/28/16 Pct Recovery = 90% Analysis Date = 03/24/16 Pct Recovery = 90% Analysis Date = 03/24/16 Pct Recovery = 90% Analysis Date = 03/19/16 Pct Recovery = 90% Analysis Date = 03/19/16 Pct Recovery = 90% Analysis Date = 03/14/16 Pct Recovery = 90% Analysis Date = 03/14/16 Pct Recovery = 90% Analysis Date = 03/09/16 Pct Recovery = 90% Analysis Date = 03/09/16 Pct Recovery = 90% Analysis Date = 03/04/16 Pct Recovery = 90% Analysis Date = 03/04/16 Pct Recovery = 90% Analysis Date = 02/29/16 Pct Recovery = 90% Analysis Date = 02/29/16 Pct Recovery = 90% Analysis Date = 02/24/16 Pct Recovery = 91% Analysis Date = 02/24/16 Pct Recovery = 91% Analysis Date = 02/19/16 Pct Recovery = 91% Analysis Date = 02/19/16 Pct Recovery = 91% Analysis Date = 02/14/16 Pct Recovery = 91% Analysis Date = 02/14/16 Pct Recovery = 91% Analysis Date = 02/10/16 Pct Recovery = 91% Analysis Date = 02/10/16 Pct Recovery = 91% Analysis Date = 02/05/16 Pct Recovery = 91% Analysis Date = 02/05/16 Pct Recovery = 91% Analysis Date = 01/31/16 Pct Recovery = 91% Analysis Date = 01/31/16 Pct Recovery = 91% Analysis Date = 01/26/16 Pct Recovery = 91% Analysis Date = 01/26/16 Pct Recovery = 91% Analysis Date = 01/21/16 Pct Recovery = 91% Analysis Date = 01/21/16 Pct Recovery = 91% Analysis Date = 01/17/16 Pct Recovery = 92% Analysis Date = 01/17/16 Pct Recovery = 92% Analysis Date = 01/12/16 Pct Recovery = 92% Analysis Date = 01/12/16 Pct Recovery = 92% Analysis Date = 01/07/16 Pct Recovery = 92% Analysis Date = 01/07/16 Pct Recovery = 92% Analysis Date = 01/02/16 Pct Recovery = 92% Analysis Date = 01/02/16 Pct Recovery = 92% Analysis Date = 12/29/15 Pct Recovery = 92% Analysis Date = 12/29/15 Pct Recovery = 92% Analysis Date = 12/24/15 Pct Recovery = 92% Analysis Date = 12/24/15 Pct Recovery = 92% Analysis Date = 12/19/15 Pct Recovery = 92% Analysis Date = 12/19/15 Pct Recovery = 92% Analysis Date = 12/14/15 Pct Recovery = 92% Analysis Date = 12/14/15 Pct Recovery = 92% Analysis Date = 12/09/15 Pct Recovery = 92% Analysis Date = 12/09/15 Pct Recovery = 92% Analysis Date = 12/05/15 Pct Recovery = 92% Analysis Date = 12/05/15 Pct Recovery = 92% Analysis Date = 11/30/15 Pct Recovery = 92% Analysis Date = 11/30/15 Pct Recovery = 92% Analysis Date = 11/25/15 Pct Recovery = 93% Analysis Date = 11/25/15 Pct Recovery = 93% Analysis Date = 11/20/15 Pct Recovery = 93% Analysis Date = 11/20/15 Pct Recovery = 93% Analysis Date = 11/16/15 Pct Recovery = 93% Analysis Date = 11/16/15 Pct Recovery = 93% Analysis Date = 11/11/15 Pct Recovery = 93% Analysis Date = 11/11/15 Pct Recovery = 93% Analysis Date = 11/06/15 Pct Recovery = 93% Analysis Date = 11/06/15 Pct Recovery = 93% Analysis Date = 11/01/15 Pct Recovery = 93% Analysis Date = 11/01/15 Pct Recovery = 93% Analysis Date = 10/27/15 Pct Recovery = 93% Analysis Date = 10/27/15 Pct Recovery = 93% Analysis Date = 10/23/15 Pct Recovery = 93% Analysis Date = 10/23/15 Pct Recovery = 93% Analysis Date = 10/18/15 Pct Recovery = 93% Analysis Date = 10/18/15 Pct Recovery = 93% Analysis Date = 10/13/15 Pct Recovery = 93% Analysis Date = 10/13/15 Pct Recovery = 93% Analysis Date = 10/08/15 Pct Recovery = 93% Analysis Date = 10/08/15 Pct Recovery = 93% Analysis Date = 10/04/15 Pct Recovery = 93% Analysis Date = 10/04/15 Pct Recovery = 93% Analysis Date = 09/29/15 Pct Recovery = 94% Analysis Date = 09/29/15 Pct Recovery = 94% Analysis Date = 09/24/15 Pct Recovery = 94% Analysis Date = 09/24/15 Pct Recovery = 94% Analysis Date = 09/19/15 Pct Recovery = 94% Analysis Date = 09/19/15 Pct Recovery = 94% Analysis Date = 09/14/15 Pct Recovery = 94% Analysis Date = 09/14/15 Pct Recovery = 94% Analysis Date = 09/10/15 Pct Recovery = 94% Analysis Date = 09/10/15 Pct Recovery = 94% Analysis Date = 09/05/15 Pct Recovery = 94% Analysis Date = 09/05/15 Pct Recovery = 94% Analysis Date = 08/31/15 Pct Recovery = 94% Analysis Date = 08/31/15 Pct Recovery = 94% Analysis Date = 08/26/15 Pct Recovery = 94% Analysis Date = 08/26/15 Pct Recovery = 94% Analysis Date = 08/21/15 Pct Recovery = 94% Analysis Date = 08/21/15 Pct Recovery = 94% Analysis Date = 08/17/15 Pct Recovery = 94% Analysis Date = 08/17/15 Pct Recovery = 94% Analysis Date = 08/12/15 Pct Recovery = 94% Analysis Date = 08/12/15 Pct Recovery = 94% Analysis Date = 08/07/15 Pct Recovery = 94% Analysis Date = 08/07/15 Pct Recovery = 94% Analysis Date = 08/02/15 Pct Recovery = 94% Analysis Date = 08/02/15 Pct Recovery = 94% Analysis Date = 07/29/15 Pct Recovery = 94% Analysis Date = 07/29/15 Pct Recovery = 94% Analysis Date = 07/24/15 Pct Recovery = 94% Analysis Date = 07/24/15 Pct Recovery = 94% Analysis Date = 07/19/15 Pct Recovery = 94% Analysis Date = 07/19/15 Pct Recovery = 94% Analysis Date = 07/14/15 Pct Recovery = 94% Analysis Date = 07/14/15 Pct Recovery = 94% Analysis Date = 07/09/15 Pct Recovery = 94% Analysis Date = 07/09/15 Pct Recovery = 94% Analysis Date = 07/05/15 Pct Recovery = 94% Analysis Date = 07/05/15 Pct Recovery = 94% Analysis Date = 06/30/15 Pct Recovery = 94% Analysis Date = 06/30/15 Pct Recovery = 94% Analysis Date = 06/25/15 Pct Recovery = 94% Analysis Date = 06/25/15 Pct Recovery = 94% Analysis Date = 06/20/15 Pct Recovery = 94% Analysis Date = 06/20/15 Pct Recovery = 94% Analysis Date = 06/16/15 Pct Recovery = 94% Analysis Date = 06/16/15 Pct Recovery = 94% Analysis Date = 06/11/15 Pct Recovery = 94% Analysis Date = 06/11/15 Pct Recovery = 94% Analysis Date = 06/06/15 Pct Recovery = 94% Analysis Date = 06/06/15 Pct Recovery = 94% Analysis Date = 06/01/15 Pct Recovery = 94% Analysis Date = 06/01/15 Pct Recovery = 94% Analysis Date = 05/27/15 Pct Recovery = 94% Analysis Date = 05/27/15 Pct Recovery = 94% Analysis Date = 05/23/15 Pct Recovery = 94% Analysis Date = 05/23/15 Pct Recovery = 94% Analysis Date = 05/18/15 Pct Recovery = 94% Analysis Date = 05/18/15 Pct Recovery = 94% Analysis Date = 05/13/15 Pct Recovery = 94% Analysis Date = 05/13/15 Pct Recovery = 94% Analysis Date = 05/08/15 Pct Recovery = 94% Analysis Date = 05/08/15 Pct Recovery = 94% Analysis Date = 05/04/15 Pct Recovery = 94% Analysis Date = 05/04/15 Pct Recovery = 94% Analysis Date = 04/29/15 Pct Recovery = 94% Analysis Date = 04/29/15 Pct Recovery = 94% Analysis Date = 04/24/15 Pct Recovery = 94% Analysis Date = 04/24/15 Pct Recovery = 94% Analysis Date = 04/19/15 Pct Recovery = 94% Analysis Date = 04/19/15 Pct Recovery = 94% Analysis Date = 04/14/15 Pct Recovery = 94% Analysis Date = 04/14/15 Pct Recovery = 94% Analysis Date = 04/10/15 Pct Recovery = 94% Analysis Date = 04/10/15 Pct Recovery = 94% Analysis Date = 04/05/15 Pct Recovery = 94% Analysis Date = 04/05/15 Pct Recovery = 94% Analysis Date = 03/31/15 Pct Recovery = 94% Analysis Date = 03/31/15 Pct Recovery = 94% Analysis Date = 03/26/15 Pct Recovery = 94% Analysis Date = 03/26/15 Pct Recovery = 94% Analysis Date = 03/22/15 Pct Recovery = 94% Analysis Date = 03/22/15 Pct Recovery = 94% Analysis Date = 03/17/15 Pct Recovery = 94% Analysis Date = 03/17/15 Pct Recovery = 94% Analysis Date = 03/12/15 Pct Recovery = 94% Analysis Date = 03/12/15 Pct Recovery = 94% Analysis Date = 03/07/15 Pct Recovery = 94% Analysis Date = 03/07/15 Pct Recovery = 94% Analysis Date = 03/02/15 Pct Recovery = 94% Analysis Date = 03/02/15 Pct Recovery = 94% Analysis Date = 02/26/15 Pct Recovery = 94% Analysis Date = 02/26/15 Pct Recovery = 94% Analysis Date = 02/21/15 Pct Recovery = 94% Analysis Date = 02/21/15 Pct Recovery = 94% Analysis Date = 02/16/15 Pct Recovery = 94% Analysis Date = 02/16/15 Pct Recovery = 94% Analysis Date = 02/11/15 Pct Recovery = 94% Analysis Date = 02/11/15 Pct Recovery = 94% Analysis Date = 02/07/15 Pct Recovery = 95% Analysis Date = 02/07/15 Pct Recovery = 95% Analysis Date = 02/02/15 Pct Recovery = 95% Analysis Date = 02/02/15 Pct Recovery = 95% Analysis Date = 01/28/15 Pct Recovery = 95% Analysis Date = 01/28/15 Pct Recovery = 95% Analysis Date = 01/23/15 Pct Recovery = 95% Analysis Date = 01/23/15 Pct Recovery = 95% Analysis Date = 01/18/15 Pct Recovery = 95% Analysis Date = 01/18/15 Pct Recovery = 95% Analysis Date = 01/14/15 Pct Recovery = 95% Analysis Date = 01/14/15 Pct Recovery = 95% Analysis Date = 01/09/15 Pct Recovery = 95% Analysis Date = 01/09/15 Pct Recovery = 95% Analysis Date = 01/04/15 Pct Recovery = 95% Analysis Date = 01/04/15 Pct Recovery = 95% Analysis Date = 12/30/14 Pct Recovery = 94% Analysis Date = 12/30/14 Pct Recovery = 94% Analysis Date = 12/25/14 Pct Recovery = 94% Analysis Date = 12/25/14 Pct Recovery = 94% Analysis Date = 12/21/14 Pct Recovery = 94% Analysis Date = 12/21/14 Pct Recovery = 94% Analysis Date = 12/16/14 Pct Recovery = 94% Analysis Date = 12/16/14 Pct Recovery = 94% Analysis Date = 12/11/14 Pct Recovery = 94% Analysis Date = 12/11/14 Pct Recovery = 94% Analysis Date = 12/06/14 Pct Recovery = 94% Analysis Date = 12/06/14 Pct Recovery = 94% Analysis Date = 12/02/14 Pct Recovery = 94% Analysis Date = 12/02/14 Pct Recovery = 94% Analysis Date = 11/27/14 Pct Recovery = 94% Analysis Date = 11/27/14 Pct Recovery = 94% Analysis Date = 11/22/14 Pct Recovery = 94% Analysis Date = 11/22/14 Pct Recovery = 94% Analysis Date = 11/17/14 Pct Recovery = 94% Analysis Date = 11/17/14 Pct Recovery = 94% Analysis Date = 11/12/14 Pct Recovery = 94% Analysis Date = 11/12/14 Pct Recovery = 94% Analysis Date = 11/08/14 Pct Recovery = 94% Analysis Date = 11/08/14 Pct Recovery = 94% Analysis Date = 11/03/14 Pct Recovery = 94% Analysis Date = 11/03/14 Pct Recovery = 94% Analysis Date = 10/29/14 Pct Recovery = 93% Analysis Date = 10/29/14 Pct Recovery = 93% Analysis Date = 10/24/14 Pct Recovery = 93% Analysis Date = 10/24/14 Pct Recovery = 93% Analysis Date = 10/20/14 Pct Recovery = 93% Analysis Date = 10/20/14 Pct Recovery = 93% Analysis Date = 10/15/14 Pct Recovery = 93% Analysis Date = 10/15/14 Pct Recovery = 93% Analysis Date = 10/10/14 Pct Recovery = 93% Analysis Date = 10/10/14 Pct Recovery = 93% Analysis Date = 10/05/14 Pct Recovery = 93% Analysis Date = 10/05/14 Pct Recovery = 93% Analysis Date = 09/30/14 Pct Recovery = 93% Analysis Date = 09/30/14 Pct Recovery = 93% Analysis Date = 09/26/14 Pct Recovery = 93% Analysis Date = 09/26/14 Pct Recovery = 93% Analysis Date = 09/21/14 Pct Recovery = 93% Analysis Date = 09/21/14 Pct Recovery = 93% Analysis Date = 09/16/14 Pct Recovery = 93% Analysis Date = 09/16/14 Pct Recovery = 93% Analysis Date = 09/11/14 Pct Recovery = 93% Analysis Date = 09/11/14 Pct Recovery = 93% Analysis Date = 09/07/14 Pct Recovery = 92% Analysis Date = 09/07/14 Pct Recovery = 92% Analysis Date = 09/02/14 Pct Recovery = 92% Analysis Date = 09/02/14 Pct Recovery = 92% Analysis Date = 08/28/14 Pct Recovery = 92% Analysis Date = 08/28/14 Pct Recovery = 92% Analysis Date = 08/23/14 Pct Recovery = 92% Analysis Date = 08/23/14 Pct Recovery = 92% Analysis Date = 08/18/14 Pct Recovery = 92% Analysis Date = 08/18/14 Pct Recovery = 92% Analysis Date = 08/14/14 Pct Recovery = 92% Analysis Date = 08/14/14 Pct Recovery = 92% Analysis Date = 08/09/14 Pct Recovery = 92% Analysis Date = 08/09/14 Pct Recovery = 92% Analysis Date = 08/04/14 Pct Recovery = 92% Analysis Date = 08/04/14 Pct Recovery = 92% Analysis Date = 07/30/14 Pct Recovery = 92% Analysis Date = 07/30/14 Pct Recovery = 92% Analysis Date = 07/26/14 Pct Recovery = 92% Analysis Date = 07/26/14 Pct Recovery = 92% Analysis Date = 07/21/14 Pct Recovery = 92% Analysis Date = 07/21/14 Pct Recovery = 92% Analysis Date = 07/16/14 Pct Recovery = 91% Analysis Date = 07/16/14 Pct Recovery = 91% Analysis Date = 07/11/14 Pct Recovery = 91% Analysis Date = 07/11/14 Pct Recovery = 91% Analysis Date = 07/06/14 Pct Recovery = 91% Analysis Date = 07/06/14 Pct Recovery = 91% Analysis Date = 07/02/14 Pct Recovery = 91% Analysis Date = 07/02/14 Pct Recovery = 91% Analysis Date = 06/27/14 Pct Recovery = 91% Analysis Date = 06/27/14 Pct Recovery = 91% Analysis Date = 06/22/14 Pct Recovery = 91% Analysis Date = 06/22/14 Pct Recovery = 91% Analysis Date = 06/17/14 Pct Recovery = 91% Analysis Date = 06/17/14 Pct Recovery = 91% Analysis Date = 06/13/14 Pct Recovery = 91% Analysis Date = 06/13/14 Pct Recovery = 91% Analysis Date = 06/08/14 Pct Recovery = 91% Analysis Date = 06/08/14 Pct Recovery = 91% Analysis Date = 06/03/14 Pct Recovery = 90% Analysis Date = 06/03/14 Pct Recovery = 90% Analysis Date = 05/29/14 Pct Recovery = 90% Analysis Date = 05/29/14 Pct Recovery = 90% Analysis Date = 05/24/14 Pct Recovery = 90% Analysis Date = 05/24/14 Pct Recovery = 90% Analysis Date = 05/20/14 Pct Recovery = 90% Analysis Date = 05/20/14 Pct Recovery = 90% Analysis Date = 05/15/14 Pct Recovery = 90% Analysis Date = 05/15/14 Pct Recovery = 90% Analysis Date = 05/10/14 Pct Recovery = 90% Analysis Date = 05/10/14 Pct Recovery = 90% Analysis Date = 05/05/14 Pct Recovery = 90% Analysis Date = 05/05/14 Pct Recovery = 90% Analysis Date = 05/01/14 Pct Recovery = 90% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
ETHYLBENZENE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 48 91% 9% 91% 7%
Total 48 91% 9% 91% 7%

Sample Statistics
ETHYLBENZENE

Characteristic N % % Basis
Plotted 48 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 48 .  
False Negatives 0 0% 0 out of 48
Not Spiked 25 .  
False Positives 0 0% 0 out of 25

BQS OBSP Determination:
ETHYL METHACRYLATE
METHOD: 4440 , TESTIDCODE: 73570GCM66
Open Data Set

Analysis Date = 08/04/16 SpikeMix = Crescent 03FF058: 40 µl & Supelco LC20141V: 40 µl Pct Recovery = 87% Analysis Date = 07/20/16 SpikeMix = Supelco LC20141V: 40 µl & Accu 216041125: 40 µl Pct Recovery = 93% Analysis Date = 12/16/16 SpikeMix = NSI 041816AVOC: 40 µl & ChemService 5082900: 40 µl Pct Recovery = 101% Analysis Date = 11/21/16 SpikeMix = Crescent 03FF058: 25 µl & Supelco LC20141V: 25 µl Pct Recovery = 96% Analysis Date = 09/08/16 SpikeMix = Supelco LC20141V: 25 µl & Accu 216041125: 25 µl Pct Recovery = 79% Analysis Date = 08/26/16 SpikeMix = NSI 041816AVOC: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 95% Analysis Date = 08/12/16 SpikeMix = ChemService 5082900: 25 µl & Phenova B20160319: 25 µl Pct Recovery = 86% Analysis Date = 06/30/16 SpikeMix = Crescent 03FF058: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 95% Analysis Date = 07/13/15 SpikeMix = Crescent 04EE008: 25 µl & NSI 050515AVOC: 25 µl Pct Recovery = 93% Analysis Date = 09/29/15 SpikeMix = Accu 215041380: 25 µl & ERA 0406-15-03: 25 µl Pct Recovery = 92% Analysis Date = 06/16/15 SpikeMix = ERA 0406-15-03: 25 µl & Supelco LC13545: 25 µl Pct Recovery = 76% Analysis Date = 10/13/16 SpikeMix = NSI 041816AVOC: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 100% Analysis Date = 05/27/16 SpikeMix = Phenova B20160319: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 85% Analysis Date = 11/29/16 SpikeMix = ChemService 5082900: 15 µl & Phenova B20160319: 15 µl Pct Recovery = 90% Analysis Date = 09/28/16 SpikeMix = Crescent 03FF058: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 94% Analysis Date = 06/30/16 SpikeMix = ChemService 5082900: 15 µl & Accu 216041125: 15 µl Pct Recovery = 92% Analysis Date = 06/10/16 SpikeMix = NSI 041816AVOC: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 84% Analysis Date = 11/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 94% Analysis Date = 10/17/15 SpikeMix = Crescent 04EE008: 15 µl & NSI 050515AVOC: 15 µl Pct Recovery = 101% Analysis Date = 06/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Accu 215041380: 15 µl Pct Recovery = 88% Analysis Date = 04/26/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 94% Analysis Date = 03/04/16 SpikeMix = Accu 215041380: 15 µl & ERA 0406-15-03: 15 µl Pct Recovery = 91% Analysis Date = 02/05/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 85% Analysis Date = 10/16/15 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 82% Analysis Date = 04/09/15 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 83% Analysis Date = 08/19/14 SpikeMix = Spex Organics C1140417015: 20 µl & Accu 214031115: 20 µl Pct Recovery = 98% Analysis Date = 07/01/14 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 94% Analysis Date = 05/01/14 SpikeMix = Accu 214031115: 20 µl & NSI 032614: 20 µl Pct Recovery = 77% Analysis Date = 03/19/15 SpikeMix = Spex Organics C1140417015: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 90% Analysis Date = 12/17/14 SpikeMix = Supelco LC06438: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 89% Analysis Date = 11/14/14 SpikeMix = Crescent 03DD004: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 93% Analysis Date = 06/10/14 SpikeMix = Crescent 03DD004: 20 µl & NSI 032614: 20 µl Pct Recovery = 78% Analysis Date = 03/17/16 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 97% Analysis Date = 01/27/16 SpikeMix = Crescent 04EE008: 10 µl & NSI 050515AVOC: 10 µl Pct Recovery = 88% Analysis Date = 12/10/15 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 110% Analysis Date = 09/03/15 SpikeMix = NSI 050515AVOC: 10 µl & Spex Organics EN150428007: 10 µl Pct Recovery = 93% Analysis Date = 11/20/15 SpikeMix = Accu 215041380: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 89% Analysis Date = 07/31/15 SpikeMix = Crescent 04EE008: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 90% Analysis Date = 06/27/15 SpikeMix = ERA 0406-15-03: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 95% Analysis Date = 01/13/15 SpikeMix = Accu 214031115: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 98% Analysis Date = 09/09/14 SpikeMix = Accu 214031115: 10 µl & NSI 032614: 10 µl Pct Recovery = 117% Analysis Date = 07/23/14 SpikeMix = Spex Organics C1140417015: 10 µl & Accu 214031115: 10 µl Pct Recovery = 103% Analysis Date = 06/18/14 SpikeMix = Supelco LC06438: 10 µl & Accu 214031115: 10 µl Pct Recovery = 110% Analysis Date = 07/29/14 SpikeMix = Crescent 03DD004: 10 µl & NSI 032614: 10 µl Pct Recovery = 101% Analysis Date = 05/03/14 SpikeMix = Crescent 03DD004: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 103% Analysis Date = 11/06/14 SpikeMix = Spex Organics C1140417015: 10 µl & Crescent 03DD004: 10 µl Pct Recovery = 113% Analysis Date = 10/04/14 SpikeMix = Crescent 03DD004: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 90% Analysis Date = 12/15/16 Pct Recovery = 93% Analysis Date = 12/11/16 Pct Recovery = 93% Analysis Date = 12/11/16 Pct Recovery = 93% Analysis Date = 12/06/16 Pct Recovery = 93% Analysis Date = 12/06/16 Pct Recovery = 93% Analysis Date = 12/01/16 Pct Recovery = 93% Analysis Date = 12/01/16 Pct Recovery = 93% Analysis Date = 11/26/16 Pct Recovery = 93% Analysis Date = 11/26/16 Pct Recovery = 93% Analysis Date = 11/21/16 Pct Recovery = 93% Analysis Date = 11/21/16 Pct Recovery = 93% Analysis Date = 11/17/16 Pct Recovery = 93% Analysis Date = 11/17/16 Pct Recovery = 93% Analysis Date = 11/12/16 Pct Recovery = 93% Analysis Date = 11/12/16 Pct Recovery = 93% Analysis Date = 11/07/16 Pct Recovery = 93% Analysis Date = 11/07/16 Pct Recovery = 93% Analysis Date = 11/02/16 Pct Recovery = 93% Analysis Date = 11/02/16 Pct Recovery = 93% Analysis Date = 10/28/16 Pct Recovery = 93% Analysis Date = 10/28/16 Pct Recovery = 93% Analysis Date = 10/24/16 Pct Recovery = 93% Analysis Date = 10/24/16 Pct Recovery = 93% Analysis Date = 10/19/16 Pct Recovery = 92% Analysis Date = 10/19/16 Pct Recovery = 92% Analysis Date = 10/14/16 Pct Recovery = 92% Analysis Date = 10/14/16 Pct Recovery = 92% Analysis Date = 10/09/16 Pct Recovery = 92% Analysis Date = 10/09/16 Pct Recovery = 92% Analysis Date = 10/04/16 Pct Recovery = 92% Analysis Date = 10/04/16 Pct Recovery = 92% Analysis Date = 09/30/16 Pct Recovery = 92% Analysis Date = 09/30/16 Pct Recovery = 92% Analysis Date = 09/25/16 Pct Recovery = 92% Analysis Date = 09/25/16 Pct Recovery = 92% Analysis Date = 09/20/16 Pct Recovery = 92% Analysis Date = 09/20/16 Pct Recovery = 92% Analysis Date = 09/15/16 Pct Recovery = 92% Analysis Date = 09/15/16 Pct Recovery = 92% Analysis Date = 09/10/16 Pct Recovery = 92% Analysis Date = 09/10/16 Pct Recovery = 92% Analysis Date = 09/06/16 Pct Recovery = 92% Analysis Date = 09/06/16 Pct Recovery = 92% Analysis Date = 09/01/16 Pct Recovery = 92% Analysis Date = 09/01/16 Pct Recovery = 92% Analysis Date = 08/27/16 Pct Recovery = 92% Analysis Date = 08/27/16 Pct Recovery = 92% Analysis Date = 08/22/16 Pct Recovery = 92% Analysis Date = 08/22/16 Pct Recovery = 92% Analysis Date = 08/17/16 Pct Recovery = 92% Analysis Date = 08/17/16 Pct Recovery = 92% Analysis Date = 08/13/16 Pct Recovery = 92% Analysis Date = 08/13/16 Pct Recovery = 92% Analysis Date = 08/08/16 Pct Recovery = 92% Analysis Date = 08/08/16 Pct Recovery = 92% Analysis Date = 08/03/16 Pct Recovery = 92% Analysis Date = 08/03/16 Pct Recovery = 92% Analysis Date = 07/29/16 Pct Recovery = 92% Analysis Date = 07/29/16 Pct Recovery = 92% Analysis Date = 07/24/16 Pct Recovery = 92% Analysis Date = 07/24/16 Pct Recovery = 92% Analysis Date = 07/20/16 Pct Recovery = 92% Analysis Date = 07/20/16 Pct Recovery = 92% Analysis Date = 07/15/16 Pct Recovery = 92% Analysis Date = 07/15/16 Pct Recovery = 92% Analysis Date = 07/10/16 Pct Recovery = 92% Analysis Date = 07/10/16 Pct Recovery = 92% Analysis Date = 07/05/16 Pct Recovery = 92% Analysis Date = 07/05/16 Pct Recovery = 92% Analysis Date = 06/30/16 Pct Recovery = 92% Analysis Date = 06/30/16 Pct Recovery = 92% Analysis Date = 06/26/16 Pct Recovery = 92% Analysis Date = 06/26/16 Pct Recovery = 92% Analysis Date = 06/21/16 Pct Recovery = 92% Analysis Date = 06/21/16 Pct Recovery = 92% Analysis Date = 06/16/16 Pct Recovery = 92% Analysis Date = 06/16/16 Pct Recovery = 92% Analysis Date = 06/11/16 Pct Recovery = 92% Analysis Date = 06/11/16 Pct Recovery = 92% Analysis Date = 06/06/16 Pct Recovery = 91% Analysis Date = 06/06/16 Pct Recovery = 91% Analysis Date = 06/02/16 Pct Recovery = 91% Analysis Date = 06/02/16 Pct Recovery = 91% Analysis Date = 05/28/16 Pct Recovery = 91% Analysis Date = 05/28/16 Pct Recovery = 91% Analysis Date = 05/23/16 Pct Recovery = 91% Analysis Date = 05/23/16 Pct Recovery = 91% Analysis Date = 05/18/16 Pct Recovery = 91% Analysis Date = 05/18/16 Pct Recovery = 91% Analysis Date = 05/13/16 Pct Recovery = 91% Analysis Date = 05/13/16 Pct Recovery = 91% Analysis Date = 05/09/16 Pct Recovery = 91% Analysis Date = 05/09/16 Pct Recovery = 91% Analysis Date = 05/04/16 Pct Recovery = 91% Analysis Date = 05/04/16 Pct Recovery = 91% Analysis Date = 04/29/16 Pct Recovery = 91% Analysis Date = 04/29/16 Pct Recovery = 91% Analysis Date = 04/24/16 Pct Recovery = 91% Analysis Date = 04/24/16 Pct Recovery = 91% Analysis Date = 04/19/16 Pct Recovery = 91% Analysis Date = 04/19/16 Pct Recovery = 91% Analysis Date = 04/15/16 Pct Recovery = 91% Analysis Date = 04/15/16 Pct Recovery = 91% Analysis Date = 04/10/16 Pct Recovery = 91% Analysis Date = 04/10/16 Pct Recovery = 91% Analysis Date = 04/05/16 Pct Recovery = 92% Analysis Date = 04/05/16 Pct Recovery = 92% Analysis Date = 03/31/16 Pct Recovery = 92% Analysis Date = 03/31/16 Pct Recovery = 92% Analysis Date = 03/26/16 Pct Recovery = 92% Analysis Date = 03/26/16 Pct Recovery = 92% Analysis Date = 03/22/16 Pct Recovery = 92% Analysis Date = 03/22/16 Pct Recovery = 92% Analysis Date = 03/17/16 Pct Recovery = 92% Analysis Date = 03/17/16 Pct Recovery = 92% Analysis Date = 03/12/16 Pct Recovery = 92% Analysis Date = 03/12/16 Pct Recovery = 92% Analysis Date = 03/07/16 Pct Recovery = 92% Analysis Date = 03/07/16 Pct Recovery = 92% Analysis Date = 03/02/16 Pct Recovery = 92% Analysis Date = 03/02/16 Pct Recovery = 92% Analysis Date = 02/27/16 Pct Recovery = 92% Analysis Date = 02/27/16 Pct Recovery = 92% Analysis Date = 02/22/16 Pct Recovery = 92% Analysis Date = 02/22/16 Pct Recovery = 92% Analysis Date = 02/17/16 Pct Recovery = 92% Analysis Date = 02/17/16 Pct Recovery = 92% Analysis Date = 02/12/16 Pct Recovery = 92% Analysis Date = 02/12/16 Pct Recovery = 92% Analysis Date = 02/07/16 Pct Recovery = 92% Analysis Date = 02/07/16 Pct Recovery = 92% Analysis Date = 02/03/16 Pct Recovery = 92% Analysis Date = 02/03/16 Pct Recovery = 92% Analysis Date = 01/29/16 Pct Recovery = 92% Analysis Date = 01/29/16 Pct Recovery = 92% Analysis Date = 01/24/16 Pct Recovery = 92% Analysis Date = 01/24/16 Pct Recovery = 92% Analysis Date = 01/19/16 Pct Recovery = 92% Analysis Date = 01/19/16 Pct Recovery = 92% Analysis Date = 01/14/16 Pct Recovery = 92% Analysis Date = 01/14/16 Pct Recovery = 92% Analysis Date = 01/10/16 Pct Recovery = 92% Analysis Date = 01/10/16 Pct Recovery = 92% Analysis Date = 01/05/16 Pct Recovery = 92% Analysis Date = 01/05/16 Pct Recovery = 92% Analysis Date = 12/31/15 Pct Recovery = 92% Analysis Date = 12/31/15 Pct Recovery = 92% Analysis Date = 12/26/15 Pct Recovery = 92% Analysis Date = 12/26/15 Pct Recovery = 92% Analysis Date = 12/21/15 Pct Recovery = 92% Analysis Date = 12/21/15 Pct Recovery = 92% Analysis Date = 12/17/15 Pct Recovery = 92% Analysis Date = 12/17/15 Pct Recovery = 92% Analysis Date = 12/12/15 Pct Recovery = 92% Analysis Date = 12/12/15 Pct Recovery = 92% Analysis Date = 12/07/15 Pct Recovery = 92% Analysis Date = 12/07/15 Pct Recovery = 92% Analysis Date = 12/02/15 Pct Recovery = 92% Analysis Date = 12/02/15 Pct Recovery = 92% Analysis Date = 11/27/15 Pct Recovery = 92% Analysis Date = 11/27/15 Pct Recovery = 92% Analysis Date = 11/23/15 Pct Recovery = 92% Analysis Date = 11/23/15 Pct Recovery = 92% Analysis Date = 11/18/15 Pct Recovery = 92% Analysis Date = 11/18/15 Pct Recovery = 92% Analysis Date = 11/13/15 Pct Recovery = 92% Analysis Date = 11/13/15 Pct Recovery = 92% Analysis Date = 11/08/15 Pct Recovery = 92% Analysis Date = 11/08/15 Pct Recovery = 92% Analysis Date = 11/03/15 Pct Recovery = 92% Analysis Date = 11/03/15 Pct Recovery = 92% Analysis Date = 10/30/15 Pct Recovery = 92% Analysis Date = 10/30/15 Pct Recovery = 92% Analysis Date = 10/25/15 Pct Recovery = 91% Analysis Date = 10/25/15 Pct Recovery = 91% Analysis Date = 10/20/15 Pct Recovery = 91% Analysis Date = 10/20/15 Pct Recovery = 91% Analysis Date = 10/15/15 Pct Recovery = 91% Analysis Date = 10/15/15 Pct Recovery = 91% Analysis Date = 10/10/15 Pct Recovery = 91% Analysis Date = 10/10/15 Pct Recovery = 91% Analysis Date = 10/06/15 Pct Recovery = 91% Analysis Date = 10/06/15 Pct Recovery = 91% Analysis Date = 10/01/15 Pct Recovery = 91% Analysis Date = 10/01/15 Pct Recovery = 91% Analysis Date = 09/26/15 Pct Recovery = 91% Analysis Date = 09/26/15 Pct Recovery = 91% Analysis Date = 09/21/15 Pct Recovery = 91% Analysis Date = 09/21/15 Pct Recovery = 91% Analysis Date = 09/16/15 Pct Recovery = 91% Analysis Date = 09/16/15 Pct Recovery = 91% Analysis Date = 09/12/15 Pct Recovery = 91% Analysis Date = 09/12/15 Pct Recovery = 91% Analysis Date = 09/07/15 Pct Recovery = 91% Analysis Date = 09/07/15 Pct Recovery = 91% Analysis Date = 09/02/15 Pct Recovery = 91% Analysis Date = 09/02/15 Pct Recovery = 91% Analysis Date = 08/28/15 Pct Recovery = 91% Analysis Date = 08/28/15 Pct Recovery = 91% Analysis Date = 08/23/15 Pct Recovery = 91% Analysis Date = 08/23/15 Pct Recovery = 91% Analysis Date = 08/19/15 Pct Recovery = 91% Analysis Date = 08/19/15 Pct Recovery = 91% Analysis Date = 08/14/15 Pct Recovery = 91% Analysis Date = 08/14/15 Pct Recovery = 91% Analysis Date = 08/09/15 Pct Recovery = 91% Analysis Date = 08/09/15 Pct Recovery = 91% Analysis Date = 08/04/15 Pct Recovery = 91% Analysis Date = 08/04/15 Pct Recovery = 91% Analysis Date = 07/30/15 Pct Recovery = 91% Analysis Date = 07/30/15 Pct Recovery = 91% Analysis Date = 07/26/15 Pct Recovery = 91% Analysis Date = 07/26/15 Pct Recovery = 91% Analysis Date = 07/21/15 Pct Recovery = 91% Analysis Date = 07/21/15 Pct Recovery = 91% Analysis Date = 07/16/15 Pct Recovery = 91% Analysis Date = 07/16/15 Pct Recovery = 91% Analysis Date = 07/11/15 Pct Recovery = 91% Analysis Date = 07/11/15 Pct Recovery = 91% Analysis Date = 07/06/15 Pct Recovery = 91% Analysis Date = 07/06/15 Pct Recovery = 91% Analysis Date = 07/02/15 Pct Recovery = 91% Analysis Date = 07/02/15 Pct Recovery = 91% Analysis Date = 06/27/15 Pct Recovery = 91% Analysis Date = 06/27/15 Pct Recovery = 91% Analysis Date = 06/22/15 Pct Recovery = 91% Analysis Date = 06/22/15 Pct Recovery = 91% Analysis Date = 06/17/15 Pct Recovery = 91% Analysis Date = 06/17/15 Pct Recovery = 91% Analysis Date = 06/12/15 Pct Recovery = 91% Analysis Date = 06/12/15 Pct Recovery = 91% Analysis Date = 06/08/15 Pct Recovery = 92% Analysis Date = 06/08/15 Pct Recovery = 92% Analysis Date = 06/03/15 Pct Recovery = 92% Analysis Date = 06/03/15 Pct Recovery = 92% Analysis Date = 05/29/15 Pct Recovery = 92% Analysis Date = 05/29/15 Pct Recovery = 92% Analysis Date = 05/24/15 Pct Recovery = 92% Analysis Date = 05/24/15 Pct Recovery = 92% Analysis Date = 05/19/15 Pct Recovery = 92% Analysis Date = 05/19/15 Pct Recovery = 92% Analysis Date = 05/15/15 Pct Recovery = 92% Analysis Date = 05/15/15 Pct Recovery = 92% Analysis Date = 05/10/15 Pct Recovery = 92% Analysis Date = 05/10/15 Pct Recovery = 92% Analysis Date = 05/05/15 Pct Recovery = 92% Analysis Date = 05/05/15 Pct Recovery = 92% Analysis Date = 04/30/15 Pct Recovery = 92% Analysis Date = 04/30/15 Pct Recovery = 92% Analysis Date = 04/25/15 Pct Recovery = 92% Analysis Date = 04/25/15 Pct Recovery = 92% Analysis Date = 04/21/15 Pct Recovery = 93% Analysis Date = 04/21/15 Pct Recovery = 93% Analysis Date = 04/16/15 Pct Recovery = 93% Analysis Date = 04/16/15 Pct Recovery = 93% Analysis Date = 04/11/15 Pct Recovery = 93% Analysis Date = 04/11/15 Pct Recovery = 93% Analysis Date = 04/06/15 Pct Recovery = 93% Analysis Date = 04/06/15 Pct Recovery = 93% Analysis Date = 04/01/15 Pct Recovery = 93% Analysis Date = 04/01/15 Pct Recovery = 93% Analysis Date = 03/28/15 Pct Recovery = 93% Analysis Date = 03/28/15 Pct Recovery = 93% Analysis Date = 03/23/15 Pct Recovery = 93% Analysis Date = 03/23/15 Pct Recovery = 93% Analysis Date = 03/18/15 Pct Recovery = 93% Analysis Date = 03/18/15 Pct Recovery = 93% Analysis Date = 03/13/15 Pct Recovery = 93% Analysis Date = 03/13/15 Pct Recovery = 93% Analysis Date = 03/08/15 Pct Recovery = 93% Analysis Date = 03/08/15 Pct Recovery = 93% Analysis Date = 03/04/15 Pct Recovery = 93% Analysis Date = 03/04/15 Pct Recovery = 93% Analysis Date = 02/27/15 Pct Recovery = 94% Analysis Date = 02/27/15 Pct Recovery = 94% Analysis Date = 02/22/15 Pct Recovery = 94% Analysis Date = 02/22/15 Pct Recovery = 94% Analysis Date = 02/17/15 Pct Recovery = 94% Analysis Date = 02/17/15 Pct Recovery = 94% Analysis Date = 02/12/15 Pct Recovery = 94% Analysis Date = 02/12/15 Pct Recovery = 94% Analysis Date = 02/08/15 Pct Recovery = 94% Analysis Date = 02/08/15 Pct Recovery = 94% Analysis Date = 02/03/15 Pct Recovery = 94% Analysis Date = 02/03/15 Pct Recovery = 94% Analysis Date = 01/29/15 Pct Recovery = 94% Analysis Date = 01/29/15 Pct Recovery = 94% Analysis Date = 01/24/15 Pct Recovery = 94% Analysis Date = 01/24/15 Pct Recovery = 94% Analysis Date = 01/19/15 Pct Recovery = 94% Analysis Date = 01/19/15 Pct Recovery = 94% Analysis Date = 01/15/15 Pct Recovery = 94% Analysis Date = 01/15/15 Pct Recovery = 94% Analysis Date = 01/10/15 Pct Recovery = 94% Analysis Date = 01/10/15 Pct Recovery = 94% Analysis Date = 01/05/15 Pct Recovery = 94% Analysis Date = 01/05/15 Pct Recovery = 94% Analysis Date = 12/31/14 Pct Recovery = 94% Analysis Date = 12/31/14 Pct Recovery = 94% Analysis Date = 12/26/14 Pct Recovery = 94% Analysis Date = 12/26/14 Pct Recovery = 94% Analysis Date = 12/22/14 Pct Recovery = 95% Analysis Date = 12/22/14 Pct Recovery = 95% Analysis Date = 12/17/14 Pct Recovery = 95% Analysis Date = 12/17/14 Pct Recovery = 95% Analysis Date = 12/12/14 Pct Recovery = 95% Analysis Date = 12/12/14 Pct Recovery = 95% Analysis Date = 12/07/14 Pct Recovery = 95% Analysis Date = 12/07/14 Pct Recovery = 95% Analysis Date = 12/02/14 Pct Recovery = 95% Analysis Date = 12/02/14 Pct Recovery = 95% Analysis Date = 11/28/14 Pct Recovery = 95% Analysis Date = 11/28/14 Pct Recovery = 95% Analysis Date = 11/23/14 Pct Recovery = 95% Analysis Date = 11/23/14 Pct Recovery = 95% Analysis Date = 11/18/14 Pct Recovery = 95% Analysis Date = 11/18/14 Pct Recovery = 95% Analysis Date = 11/13/14 Pct Recovery = 95% Analysis Date = 11/13/14 Pct Recovery = 95% Analysis Date = 11/08/14 Pct Recovery = 95% Analysis Date = 11/08/14 Pct Recovery = 95% Analysis Date = 11/04/14 Pct Recovery = 95% Analysis Date = 11/04/14 Pct Recovery = 95% Analysis Date = 10/30/14 Pct Recovery = 95% Analysis Date = 10/30/14 Pct Recovery = 95% Analysis Date = 10/25/14 Pct Recovery = 95% Analysis Date = 10/25/14 Pct Recovery = 95% Analysis Date = 10/20/14 Pct Recovery = 95% Analysis Date = 10/20/14 Pct Recovery = 95% Analysis Date = 10/15/14 Pct Recovery = 96% Analysis Date = 10/15/14 Pct Recovery = 96% Analysis Date = 10/11/14 Pct Recovery = 96% Analysis Date = 10/11/14 Pct Recovery = 96% Analysis Date = 10/06/14 Pct Recovery = 96% Analysis Date = 10/06/14 Pct Recovery = 96% Analysis Date = 10/01/14 Pct Recovery = 96% Analysis Date = 10/01/14 Pct Recovery = 96% Analysis Date = 09/26/14 Pct Recovery = 96% Analysis Date = 09/26/14 Pct Recovery = 96% Analysis Date = 09/21/14 Pct Recovery = 96% Analysis Date = 09/21/14 Pct Recovery = 96% Analysis Date = 09/17/14 Pct Recovery = 96% Analysis Date = 09/17/14 Pct Recovery = 96% Analysis Date = 09/12/14 Pct Recovery = 96% Analysis Date = 09/12/14 Pct Recovery = 96% Analysis Date = 09/07/14 Pct Recovery = 96% Analysis Date = 09/07/14 Pct Recovery = 96% Analysis Date = 09/02/14 Pct Recovery = 96% Analysis Date = 09/02/14 Pct Recovery = 96% Analysis Date = 08/28/14 Pct Recovery = 96% Analysis Date = 08/28/14 Pct Recovery = 96% Analysis Date = 08/24/14 Pct Recovery = 96% Analysis Date = 08/24/14 Pct Recovery = 96% Analysis Date = 08/19/14 Pct Recovery = 96% Analysis Date = 08/19/14 Pct Recovery = 96% Analysis Date = 08/14/14 Pct Recovery = 97% Analysis Date = 08/14/14 Pct Recovery = 97% Analysis Date = 08/09/14 Pct Recovery = 97% Analysis Date = 08/09/14 Pct Recovery = 97% Analysis Date = 08/04/14 Pct Recovery = 97% Analysis Date = 08/04/14 Pct Recovery = 97% Analysis Date = 07/31/14 Pct Recovery = 97% Analysis Date = 07/31/14 Pct Recovery = 97% Analysis Date = 07/26/14 Pct Recovery = 97% Analysis Date = 07/26/14 Pct Recovery = 97% Analysis Date = 07/21/14 Pct Recovery = 97% Analysis Date = 07/21/14 Pct Recovery = 97% Analysis Date = 07/16/14 Pct Recovery = 97% Analysis Date = 07/16/14 Pct Recovery = 97% Analysis Date = 07/11/14 Pct Recovery = 97% Analysis Date = 07/11/14 Pct Recovery = 97% Analysis Date = 07/07/14 Pct Recovery = 97% Analysis Date = 07/07/14 Pct Recovery = 97% Analysis Date = 07/02/14 Pct Recovery = 97% Analysis Date = 07/02/14 Pct Recovery = 97% Analysis Date = 06/27/14 Pct Recovery = 97% Analysis Date = 06/27/14 Pct Recovery = 97% Analysis Date = 06/22/14 Pct Recovery = 97% Analysis Date = 06/22/14 Pct Recovery = 97% Analysis Date = 06/17/14 Pct Recovery = 97% Analysis Date = 06/17/14 Pct Recovery = 97% Analysis Date = 06/13/14 Pct Recovery = 97% Analysis Date = 06/13/14 Pct Recovery = 97% Analysis Date = 06/08/14 Pct Recovery = 97% Analysis Date = 06/08/14 Pct Recovery = 97% Analysis Date = 06/03/14 Pct Recovery = 97% Analysis Date = 06/03/14 Pct Recovery = 97% Analysis Date = 05/29/14 Pct Recovery = 98% Analysis Date = 05/29/14 Pct Recovery = 98% Analysis Date = 05/24/14 Pct Recovery = 98% Analysis Date = 05/24/14 Pct Recovery = 98% Analysis Date = 05/20/14 Pct Recovery = 98% Analysis Date = 05/20/14 Pct Recovery = 98% Analysis Date = 05/15/14 Pct Recovery = 98% Analysis Date = 05/15/14 Pct Recovery = 98% Analysis Date = 05/10/14 Pct Recovery = 98% Analysis Date = 05/10/14 Pct Recovery = 98% Analysis Date = 05/05/14 Pct Recovery = 98% Analysis Date = 05/05/14 Pct Recovery = 98% Analysis Date = 05/01/14 Pct Recovery = 98% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
ETHYL METHACRYLATE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 2 102% 16% 102% 17%
>= Reporting Level 45 93% 9% 93% 7%
Total 47 93% 9% 93% 7%

Sample Statistics
ETHYL METHACRYLATE

Characteristic N % % Basis
Plotted 47 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 47 .  
False Negatives 0 0% 0 out of 47
Not Spiked 26 .  
False Positives 0 0% 0 out of 26

BQS OBSP Determination:
ETHYL TERT-BUTYL ETHER
METHOD: 4440 , TESTIDCODE: 50004GCM66
Open Data Set

Analysis Date = 12/16/16 SpikeMix = NSI 041816AVOC: 40 µl & ChemService 5082900: 40 µl Pct Recovery = 94% Analysis Date = 08/04/16 SpikeMix = Crescent 03FF058: 40 µl & Supelco LC20141V: 40 µl Pct Recovery = 75% Analysis Date = 07/20/16 SpikeMix = Supelco LC20141V: 40 µl & Accu 216041125: 40 µl Pct Recovery = 85% Analysis Date = 08/31/16 SpikeMix = NSI 041816AVOC: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 95% Analysis Date = 08/12/16 SpikeMix = ChemService 5082900: 25 µl & Phenova B20160319: 25 µl Pct Recovery = 99% Analysis Date = 06/30/16 SpikeMix = Crescent 03FF058: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 104% Analysis Date = 11/21/16 SpikeMix = Crescent 03FF058: 25 µl & Supelco LC20141V: 25 µl Pct Recovery = 88% Analysis Date = 09/08/16 SpikeMix = Supelco LC20141V: 25 µl & Accu 216041125: 25 µl Pct Recovery = 85% Analysis Date = 03/19/15 SpikeMix = Spex Organics C1140417015: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 103% Analysis Date = 03/06/15 SpikeMix = ERA 0227-14-06.1A: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 102% Analysis Date = 12/17/14 SpikeMix = Supelco LC06438: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 95% Analysis Date = 11/22/14 SpikeMix = NSI 032614: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 103% Analysis Date = 09/21/14 SpikeMix = Supelco LC06438: 20 µl Pct Recovery = 129% Analysis Date = 08/19/14 SpikeMix = Spex Organics C1140417015: 20 µl & Accu 214031115: 20 µl Pct Recovery = 95% Analysis Date = 08/16/14 SpikeMix = ERA 0227-14-06.1A: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 94% Analysis Date = 06/10/14 SpikeMix = NSI 032614: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 100% Analysis Date = 09/29/15 SpikeMix = Accu 215041380: 25 µl & ERA 0406-15-03: 25 µl Pct Recovery = 97% Analysis Date = 06/16/15 SpikeMix = ERA 0406-15-03: 25 µl & Supelco LC13545: 25 µl Pct Recovery = 86% Analysis Date = 07/13/15 SpikeMix = Crescent 04EE008: 25 µl & NSI 050515AVOC: 25 µl Pct Recovery = 85% Analysis Date = 11/29/16 SpikeMix = ChemService 5082900: 15 µl & Phenova B20160319: 15 µl Pct Recovery = 107% Analysis Date = 09/28/16 SpikeMix = Crescent 03FF058: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 109% Analysis Date = 06/30/16 SpikeMix = ChemService 5082900: 15 µl & Accu 216041125: 15 µl Pct Recovery = 107% Analysis Date = 06/10/16 SpikeMix = NSI 041816AVOC: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 90% Analysis Date = 10/13/16 SpikeMix = NSI 041816AVOC: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 103% Analysis Date = 05/27/16 SpikeMix = Phenova B20160319: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 107% Analysis Date = 04/26/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 144% Analysis Date = 03/04/16 SpikeMix = Accu 215041380: 15 µl & ERA 0406-15-03: 15 µl Pct Recovery = 111% Analysis Date = 02/05/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 109% Analysis Date = 10/16/15 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 126% Analysis Date = 11/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 92% Analysis Date = 10/17/15 SpikeMix = Crescent 04EE008: 15 µl & NSI 050515AVOC: 15 µl Pct Recovery = 81% Analysis Date = 06/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Accu 215041380: 15 µl Pct Recovery = 87% Analysis Date = 11/06/14 SpikeMix = Spex Organics C1140417015: 10 µl & Crescent 03DD004: 10 µl Pct Recovery = 112% Analysis Date = 10/21/14 SpikeMix = ERA 0227-14-06.1A: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 115% Analysis Date = 09/09/14 SpikeMix = NSI 032614: 10 µl & Spex Organics C1140417015: 10 µl Pct Recovery = 108% Analysis Date = 07/23/14 SpikeMix = Spex Organics C1140417015: 10 µl & Accu 214031115: 10 µl Pct Recovery = 100% Analysis Date = 07/11/14 SpikeMix = Spex Organics C1140417015: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 104% Analysis Date = 06/18/14 SpikeMix = Supelco LC06438: 10 µl & Accu 214031115: 10 µl Pct Recovery = 117% Analysis Date = 05/30/14 SpikeMix = NSI 032614: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 98% Analysis Date = 05/03/14 SpikeMix = Crescent 03DD004: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 98% Analysis Date = 11/20/15 SpikeMix = Accu 215041380: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 124% Analysis Date = 08/07/15 SpikeMix = Crescent 04EE008: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 116% Analysis Date = 06/27/15 SpikeMix = ERA 0406-15-03: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 125% Analysis Date = 03/17/16 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 81% Analysis Date = 01/27/16 SpikeMix = Crescent 04EE008: 10 µl & NSI 050515AVOC: 10 µl Pct Recovery = 75% Analysis Date = 12/10/15 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 89% Analysis Date = 09/03/15 SpikeMix = NSI 050515AVOC: 10 µl & Spex Organics EN150428007: 10 µl Pct Recovery = 77% Analysis Date = 12/16/16 Pct Recovery = 95% Analysis Date = 12/11/16 Pct Recovery = 96% Analysis Date = 12/11/16 Pct Recovery = 96% Analysis Date = 12/06/16 Pct Recovery = 96% Analysis Date = 12/06/16 Pct Recovery = 96% Analysis Date = 12/01/16 Pct Recovery = 96% Analysis Date = 12/01/16 Pct Recovery = 96% Analysis Date = 11/26/16 Pct Recovery = 96% Analysis Date = 11/26/16 Pct Recovery = 96% Analysis Date = 11/22/16 Pct Recovery = 96% Analysis Date = 11/22/16 Pct Recovery = 96% Analysis Date = 11/17/16 Pct Recovery = 96% Analysis Date = 11/17/16 Pct Recovery = 96% Analysis Date = 11/12/16 Pct Recovery = 96% Analysis Date = 11/12/16 Pct Recovery = 96% Analysis Date = 11/07/16 Pct Recovery = 96% Analysis Date = 11/07/16 Pct Recovery = 96% Analysis Date = 11/02/16 Pct Recovery = 96% Analysis Date = 11/02/16 Pct Recovery = 96% Analysis Date = 10/29/16 Pct Recovery = 96% Analysis Date = 10/29/16 Pct Recovery = 96% Analysis Date = 10/24/16 Pct Recovery = 96% Analysis Date = 10/24/16 Pct Recovery = 96% Analysis Date = 10/19/16 Pct Recovery = 97% Analysis Date = 10/19/16 Pct Recovery = 97% Analysis Date = 10/14/16 Pct Recovery = 97% Analysis Date = 10/14/16 Pct Recovery = 97% Analysis Date = 10/09/16 Pct Recovery = 97% Analysis Date = 10/09/16 Pct Recovery = 97% Analysis Date = 10/05/16 Pct Recovery = 97% Analysis Date = 10/05/16 Pct Recovery = 97% Analysis Date = 09/30/16 Pct Recovery = 97% Analysis Date = 09/30/16 Pct Recovery = 97% Analysis Date = 09/25/16 Pct Recovery = 97% Analysis Date = 09/25/16 Pct Recovery = 97% Analysis Date = 09/20/16 Pct Recovery = 97% Analysis Date = 09/20/16 Pct Recovery = 97% Analysis Date = 09/15/16 Pct Recovery = 97% Analysis Date = 09/15/16 Pct Recovery = 97% Analysis Date = 09/11/16 Pct Recovery = 97% Analysis Date = 09/11/16 Pct Recovery = 97% Analysis Date = 09/06/16 Pct Recovery = 97% Analysis Date = 09/06/16 Pct Recovery = 97% Analysis Date = 09/01/16 Pct Recovery = 98% Analysis Date = 09/01/16 Pct Recovery = 98% Analysis Date = 08/27/16 Pct Recovery = 98% Analysis Date = 08/27/16 Pct Recovery = 98% Analysis Date = 08/23/16 Pct Recovery = 98% Analysis Date = 08/23/16 Pct Recovery = 98% Analysis Date = 08/18/16 Pct Recovery = 98% Analysis Date = 08/18/16 Pct Recovery = 98% Analysis Date = 08/13/16 Pct Recovery = 98% Analysis Date = 08/13/16 Pct Recovery = 98% Analysis Date = 08/08/16 Pct Recovery = 98% Analysis Date = 08/08/16 Pct Recovery = 98% Analysis Date = 08/03/16 Pct Recovery = 98% Analysis Date = 08/03/16 Pct Recovery = 98% Analysis Date = 07/30/16 Pct Recovery = 98% Analysis Date = 07/30/16 Pct Recovery = 98% Analysis Date = 07/25/16 Pct Recovery = 98% Analysis Date = 07/25/16 Pct Recovery = 98% Analysis Date = 07/20/16 Pct Recovery = 98% Analysis Date = 07/20/16 Pct Recovery = 98% Analysis Date = 07/15/16 Pct Recovery = 98% Analysis Date = 07/15/16 Pct Recovery = 98% Analysis Date = 07/10/16 Pct Recovery = 98% Analysis Date = 07/10/16 Pct Recovery = 98% Analysis Date = 07/06/16 Pct Recovery = 98% Analysis Date = 07/06/16 Pct Recovery = 98% Analysis Date = 07/01/16 Pct Recovery = 98% Analysis Date = 07/01/16 Pct Recovery = 98% Analysis Date = 06/26/16 Pct Recovery = 99% Analysis Date = 06/26/16 Pct Recovery = 99% Analysis Date = 06/21/16 Pct Recovery = 99% Analysis Date = 06/21/16 Pct Recovery = 99% Analysis Date = 06/16/16 Pct Recovery = 99% Analysis Date = 06/16/16 Pct Recovery = 99% Analysis Date = 06/12/16 Pct Recovery = 99% Analysis Date = 06/12/16 Pct Recovery = 99% Analysis Date = 06/07/16 Pct Recovery = 99% Analysis Date = 06/07/16 Pct Recovery = 99% Analysis Date = 06/02/16 Pct Recovery = 99% Analysis Date = 06/02/16 Pct Recovery = 99% Analysis Date = 05/28/16 Pct Recovery = 99% Analysis Date = 05/28/16 Pct Recovery = 99% Analysis Date = 05/24/16 Pct Recovery = 99% Analysis Date = 05/24/16 Pct Recovery = 99% Analysis Date = 05/19/16 Pct Recovery = 99% Analysis Date = 05/19/16 Pct Recovery = 99% Analysis Date = 05/14/16 Pct Recovery = 99% Analysis Date = 05/14/16 Pct Recovery = 99% Analysis Date = 05/09/16 Pct Recovery = 99% Analysis Date = 05/09/16 Pct Recovery = 99% Analysis Date = 05/04/16 Pct Recovery = 99% Analysis Date = 05/04/16 Pct Recovery = 99% Analysis Date = 04/30/16 Pct Recovery = 99% Analysis Date = 04/30/16 Pct Recovery = 99% Analysis Date = 04/25/16 Pct Recovery = 99% Analysis Date = 04/25/16 Pct Recovery = 99% Analysis Date = 04/20/16 Pct Recovery = 99% Analysis Date = 04/20/16 Pct Recovery = 99% Analysis Date = 04/15/16 Pct Recovery = 99% Analysis Date = 04/15/16 Pct Recovery = 99% Analysis Date = 04/10/16 Pct Recovery = 100% Analysis Date = 04/10/16 Pct Recovery = 100% Analysis Date = 04/06/16 Pct Recovery = 100% Analysis Date = 04/06/16 Pct Recovery = 100% Analysis Date = 04/01/16 Pct Recovery = 100% Analysis Date = 04/01/16 Pct Recovery = 100% Analysis Date = 03/27/16 Pct Recovery = 100% Analysis Date = 03/27/16 Pct Recovery = 100% Analysis Date = 03/22/16 Pct Recovery = 100% Analysis Date = 03/22/16 Pct Recovery = 100% Analysis Date = 03/17/16 Pct Recovery = 100% Analysis Date = 03/17/16 Pct Recovery = 100% Analysis Date = 03/13/16 Pct Recovery = 100% Analysis Date = 03/13/16 Pct Recovery = 100% Analysis Date = 03/08/16 Pct Recovery = 100% Analysis Date = 03/08/16 Pct Recovery = 100% Analysis Date = 03/03/16 Pct Recovery = 100% Analysis Date = 03/03/16 Pct Recovery = 100% Analysis Date = 02/27/16 Pct Recovery = 100% Analysis Date = 02/27/16 Pct Recovery = 100% Analysis Date = 02/23/16 Pct Recovery = 100% Analysis Date = 02/23/16 Pct Recovery = 100% Analysis Date = 02/18/16 Pct Recovery = 100% Analysis Date = 02/18/16 Pct Recovery = 100% Analysis Date = 02/13/16 Pct Recovery = 100% Analysis Date = 02/13/16 Pct Recovery = 100% Analysis Date = 02/08/16 Pct Recovery = 101% Analysis Date = 02/08/16 Pct Recovery = 101% Analysis Date = 02/03/16 Pct Recovery = 101% Analysis Date = 02/03/16 Pct Recovery = 101% Analysis Date = 01/30/16 Pct Recovery = 101% Analysis Date = 01/30/16 Pct Recovery = 101% Analysis Date = 01/25/16 Pct Recovery = 100% Analysis Date = 01/25/16 Pct Recovery = 100% Analysis Date = 01/20/16 Pct Recovery = 100% Analysis Date = 01/20/16 Pct Recovery = 100% Analysis Date = 01/15/16 Pct Recovery = 100% Analysis Date = 01/15/16 Pct Recovery = 100% Analysis Date = 01/10/16 Pct Recovery = 100% Analysis Date = 01/10/16 Pct Recovery = 100% Analysis Date = 01/06/16 Pct Recovery = 100% Analysis Date = 01/06/16 Pct Recovery = 100% Analysis Date = 01/01/16 Pct Recovery = 100% Analysis Date = 01/01/16 Pct Recovery = 100% Analysis Date = 12/27/15 Pct Recovery = 100% Analysis Date = 12/27/15 Pct Recovery = 100% Analysis Date = 12/22/15 Pct Recovery = 100% Analysis Date = 12/22/15 Pct Recovery = 100% Analysis Date = 12/17/15 Pct Recovery = 100% Analysis Date = 12/17/15 Pct Recovery = 100% Analysis Date = 12/13/15 Pct Recovery = 100% Analysis Date = 12/13/15 Pct Recovery = 100% Analysis Date = 12/08/15 Pct Recovery = 100% Analysis Date = 12/08/15 Pct Recovery = 100% Analysis Date = 12/03/15 Pct Recovery = 100% Analysis Date = 12/03/15 Pct Recovery = 100% Analysis Date = 11/28/15 Pct Recovery = 100% Analysis Date = 11/28/15 Pct Recovery = 100% Analysis Date = 11/24/15 Pct Recovery = 100% Analysis Date = 11/24/15 Pct Recovery = 100% Analysis Date = 11/19/15 Pct Recovery = 100% Analysis Date = 11/19/15 Pct Recovery = 100% Analysis Date = 11/14/15 Pct Recovery = 100% Analysis Date = 11/14/15 Pct Recovery = 100% Analysis Date = 11/09/15 Pct Recovery = 100% Analysis Date = 11/09/15 Pct Recovery = 100% Analysis Date = 11/04/15 Pct Recovery = 100% Analysis Date = 11/04/15 Pct Recovery = 100% Analysis Date = 10/31/15 Pct Recovery = 100% Analysis Date = 10/31/15 Pct Recovery = 100% Analysis Date = 10/26/15 Pct Recovery = 99% Analysis Date = 10/26/15 Pct Recovery = 99% Analysis Date = 10/21/15 Pct Recovery = 99% Analysis Date = 10/21/15 Pct Recovery = 99% Analysis Date = 10/16/15 Pct Recovery = 99% Analysis Date = 10/16/15 Pct Recovery = 99% Analysis Date = 10/11/15 Pct Recovery = 99% Analysis Date = 10/11/15 Pct Recovery = 99% Analysis Date = 10/07/15 Pct Recovery = 99% Analysis Date = 10/07/15 Pct Recovery = 99% Analysis Date = 10/02/15 Pct Recovery = 99% Analysis Date = 10/02/15 Pct Recovery = 99% Analysis Date = 09/27/15 Pct Recovery = 99% Analysis Date = 09/27/15 Pct Recovery = 99% Analysis Date = 09/22/15 Pct Recovery = 99% Analysis Date = 09/22/15 Pct Recovery = 99% Analysis Date = 09/17/15 Pct Recovery = 99% Analysis Date = 09/17/15 Pct Recovery = 99% Analysis Date = 09/13/15 Pct Recovery = 99% Analysis Date = 09/13/15 Pct Recovery = 99% Analysis Date = 09/08/15 Pct Recovery = 99% Analysis Date = 09/08/15 Pct Recovery = 99% Analysis Date = 09/03/15 Pct Recovery = 99% Analysis Date = 09/03/15 Pct Recovery = 99% Analysis Date = 08/29/15 Pct Recovery = 99% Analysis Date = 08/29/15 Pct Recovery = 99% Analysis Date = 08/25/15 Pct Recovery = 99% Analysis Date = 08/25/15 Pct Recovery = 99% Analysis Date = 08/20/15 Pct Recovery = 99% Analysis Date = 08/20/15 Pct Recovery = 99% Analysis Date = 08/15/15 Pct Recovery = 99% Analysis Date = 08/15/15 Pct Recovery = 99% Analysis Date = 08/10/15 Pct Recovery = 99% Analysis Date = 08/10/15 Pct Recovery = 99% Analysis Date = 08/05/15 Pct Recovery = 99% Analysis Date = 08/05/15 Pct Recovery = 99% Analysis Date = 08/01/15 Pct Recovery = 99% Analysis Date = 08/01/15 Pct Recovery = 99% Analysis Date = 07/27/15 Pct Recovery = 99% Analysis Date = 07/27/15 Pct Recovery = 99% Analysis Date = 07/22/15 Pct Recovery = 99% Analysis Date = 07/22/15 Pct Recovery = 99% Analysis Date = 07/17/15 Pct Recovery = 99% Analysis Date = 07/17/15 Pct Recovery = 99% Analysis Date = 07/12/15 Pct Recovery = 99% Analysis Date = 07/12/15 Pct Recovery = 99% Analysis Date = 07/08/15 Pct Recovery = 100% Analysis Date = 07/08/15 Pct Recovery = 100% Analysis Date = 07/03/15 Pct Recovery = 100% Analysis Date = 07/03/15 Pct Recovery = 100% Analysis Date = 06/28/15 Pct Recovery = 100% Analysis Date = 06/28/15 Pct Recovery = 100% Analysis Date = 06/23/15 Pct Recovery = 100% Analysis Date = 06/23/15 Pct Recovery = 100% Analysis Date = 06/18/15 Pct Recovery = 100% Analysis Date = 06/18/15 Pct Recovery = 100% Analysis Date = 06/14/15 Pct Recovery = 100% Analysis Date = 06/14/15 Pct Recovery = 100% Analysis Date = 06/09/15 Pct Recovery = 100% Analysis Date = 06/09/15 Pct Recovery = 100% Analysis Date = 06/04/15 Pct Recovery = 100% Analysis Date = 06/04/15 Pct Recovery = 100% Analysis Date = 05/30/15 Pct Recovery = 100% Analysis Date = 05/30/15 Pct Recovery = 100% Analysis Date = 05/25/15 Pct Recovery = 100% Analysis Date = 05/25/15 Pct Recovery = 100% Analysis Date = 05/21/15 Pct Recovery = 100% Analysis Date = 05/21/15 Pct Recovery = 100% Analysis Date = 05/16/15 Pct Recovery = 101% Analysis Date = 05/16/15 Pct Recovery = 101% Analysis Date = 05/11/15 Pct Recovery = 101% Analysis Date = 05/11/15 Pct Recovery = 101% Analysis Date = 05/06/15 Pct Recovery = 101% Analysis Date = 05/06/15 Pct Recovery = 101% Analysis Date = 05/02/15 Pct Recovery = 101% Analysis Date = 05/02/15 Pct Recovery = 101% Analysis Date = 04/27/15 Pct Recovery = 101% Analysis Date = 04/27/15 Pct Recovery = 101% Analysis Date = 04/22/15 Pct Recovery = 101% Analysis Date = 04/22/15 Pct Recovery = 101% Analysis Date = 04/17/15 Pct Recovery = 101% Analysis Date = 04/17/15 Pct Recovery = 101% Analysis Date = 04/12/15 Pct Recovery = 101% Analysis Date = 04/12/15 Pct Recovery = 101% Analysis Date = 04/08/15 Pct Recovery = 101% Analysis Date = 04/08/15 Pct Recovery = 101% Analysis Date = 04/03/15 Pct Recovery = 101% Analysis Date = 04/03/15 Pct Recovery = 101% Analysis Date = 03/29/15 Pct Recovery = 102% Analysis Date = 03/29/15 Pct Recovery = 102% Analysis Date = 03/24/15 Pct Recovery = 102% Analysis Date = 03/24/15 Pct Recovery = 102% Analysis Date = 03/19/15 Pct Recovery = 102% Analysis Date = 03/19/15 Pct Recovery = 102% Analysis Date = 03/15/15 Pct Recovery = 102% Analysis Date = 03/15/15 Pct Recovery = 102% Analysis Date = 03/10/15 Pct Recovery = 102% Analysis Date = 03/10/15 Pct Recovery = 102% Analysis Date = 03/05/15 Pct Recovery = 102% Analysis Date = 03/05/15 Pct Recovery = 102% Analysis Date = 02/28/15 Pct Recovery = 102% Analysis Date = 02/28/15 Pct Recovery = 102% Analysis Date = 02/23/15 Pct Recovery = 102% Analysis Date = 02/23/15 Pct Recovery = 102% Analysis Date = 02/19/15 Pct Recovery = 102% Analysis Date = 02/19/15 Pct Recovery = 102% Analysis Date = 02/14/15 Pct Recovery = 102% Analysis Date = 02/14/15 Pct Recovery = 102% Analysis Date = 02/09/15 Pct Recovery = 102% Analysis Date = 02/09/15 Pct Recovery = 102% Analysis Date = 02/04/15 Pct Recovery = 102% Analysis Date = 02/04/15 Pct Recovery = 102% Analysis Date = 01/31/15 Pct Recovery = 102% Analysis Date = 01/31/15 Pct Recovery = 102% Analysis Date = 01/26/15 Pct Recovery = 103% Analysis Date = 01/26/15 Pct Recovery = 103% Analysis Date = 01/21/15 Pct Recovery = 103% Analysis Date = 01/21/15 Pct Recovery = 103% Analysis Date = 01/16/15 Pct Recovery = 103% Analysis Date = 01/16/15 Pct Recovery = 103% Analysis Date = 01/11/15 Pct Recovery = 103% Analysis Date = 01/11/15 Pct Recovery = 103% Analysis Date = 01/07/15 Pct Recovery = 103% Analysis Date = 01/07/15 Pct Recovery = 103% Analysis Date = 01/02/15 Pct Recovery = 103% Analysis Date = 01/02/15 Pct Recovery = 103% Analysis Date = 12/28/14 Pct Recovery = 103% Analysis Date = 12/28/14 Pct Recovery = 103% Analysis Date = 12/23/14 Pct Recovery = 103% Analysis Date = 12/23/14 Pct Recovery = 103% Analysis Date = 12/18/14 Pct Recovery = 103% Analysis Date = 12/18/14 Pct Recovery = 103% Analysis Date = 12/14/14 Pct Recovery = 103% Analysis Date = 12/14/14 Pct Recovery = 103% Analysis Date = 12/09/14 Pct Recovery = 103% Analysis Date = 12/09/14 Pct Recovery = 103% Analysis Date = 12/04/14 Pct Recovery = 103% Analysis Date = 12/04/14 Pct Recovery = 103% Analysis Date = 11/29/14 Pct Recovery = 103% Analysis Date = 11/29/14 Pct Recovery = 103% Analysis Date = 11/24/14 Pct Recovery = 103% Analysis Date = 11/24/14 Pct Recovery = 103% Analysis Date = 11/20/14 Pct Recovery = 103% Analysis Date = 11/20/14 Pct Recovery = 103% Analysis Date = 11/15/14 Pct Recovery = 103% Analysis Date = 11/15/14 Pct Recovery = 103% Analysis Date = 11/10/14 Pct Recovery = 103% Analysis Date = 11/10/14 Pct Recovery = 103% Analysis Date = 11/05/14 Pct Recovery = 103% Analysis Date = 11/05/14 Pct Recovery = 103% Analysis Date = 11/01/14 Pct Recovery = 104% Analysis Date = 11/01/14 Pct Recovery = 104% Analysis Date = 10/27/14 Pct Recovery = 104% Analysis Date = 10/27/14 Pct Recovery = 104% Analysis Date = 10/22/14 Pct Recovery = 104% Analysis Date = 10/22/14 Pct Recovery = 104% Analysis Date = 10/17/14 Pct Recovery = 104% Analysis Date = 10/17/14 Pct Recovery = 104% Analysis Date = 10/12/14 Pct Recovery = 104% Analysis Date = 10/12/14 Pct Recovery = 104% Analysis Date = 10/08/14 Pct Recovery = 104% Analysis Date = 10/08/14 Pct Recovery = 104% Analysis Date = 10/03/14 Pct Recovery = 104% Analysis Date = 10/03/14 Pct Recovery = 104% Analysis Date = 09/28/14 Pct Recovery = 104% Analysis Date = 09/28/14 Pct Recovery = 104% Analysis Date = 09/23/14 Pct Recovery = 104% Analysis Date = 09/23/14 Pct Recovery = 104% Analysis Date = 09/18/14 Pct Recovery = 104% Analysis Date = 09/18/14 Pct Recovery = 104% Analysis Date = 09/14/14 Pct Recovery = 104% Analysis Date = 09/14/14 Pct Recovery = 104% Analysis Date = 09/09/14 Pct Recovery = 104% Analysis Date = 09/09/14 Pct Recovery = 104% Analysis Date = 09/04/14 Pct Recovery = 104% Analysis Date = 09/04/14 Pct Recovery = 104% Analysis Date = 08/30/14 Pct Recovery = 104% Analysis Date = 08/30/14 Pct Recovery = 104% Analysis Date = 08/25/14 Pct Recovery = 104% Analysis Date = 08/25/14 Pct Recovery = 104% Analysis Date = 08/21/14 Pct Recovery = 104% Analysis Date = 08/21/14 Pct Recovery = 104% Analysis Date = 08/16/14 Pct Recovery = 104% Analysis Date = 08/16/14 Pct Recovery = 104% Analysis Date = 08/11/14 Pct Recovery = 104% Analysis Date = 08/11/14 Pct Recovery = 104% Analysis Date = 08/06/14 Pct Recovery = 104% Analysis Date = 08/06/14 Pct Recovery = 104% Analysis Date = 08/02/14 Pct Recovery = 104% Analysis Date = 08/02/14 Pct Recovery = 104% Analysis Date = 07/28/14 Pct Recovery = 104% Analysis Date = 07/28/14 Pct Recovery = 104% Analysis Date = 07/23/14 Pct Recovery = 105% Analysis Date = 07/23/14 Pct Recovery = 105% Analysis Date = 07/18/14 Pct Recovery = 105% Analysis Date = 07/18/14 Pct Recovery = 105% Analysis Date = 07/13/14 Pct Recovery = 105% Analysis Date = 07/13/14 Pct Recovery = 105% Analysis Date = 07/09/14 Pct Recovery = 105% Analysis Date = 07/09/14 Pct Recovery = 105% Analysis Date = 07/04/14 Pct Recovery = 105% Analysis Date = 07/04/14 Pct Recovery = 105% Analysis Date = 06/29/14 Pct Recovery = 105% Analysis Date = 06/29/14 Pct Recovery = 105% Analysis Date = 06/24/14 Pct Recovery = 105% Analysis Date = 06/24/14 Pct Recovery = 105% Analysis Date = 06/19/14 Pct Recovery = 105% Analysis Date = 06/19/14 Pct Recovery = 105% Analysis Date = 06/15/14 Pct Recovery = 105% Analysis Date = 06/15/14 Pct Recovery = 105% Analysis Date = 06/10/14 Pct Recovery = 105% Analysis Date = 06/10/14 Pct Recovery = 105% Analysis Date = 06/05/14 Pct Recovery = 105% Analysis Date = 06/05/14 Pct Recovery = 105% Analysis Date = 05/31/14 Pct Recovery = 105% Analysis Date = 05/31/14 Pct Recovery = 105% Analysis Date = 05/26/14 Pct Recovery = 105% Analysis Date = 05/26/14 Pct Recovery = 105% Analysis Date = 05/22/14 Pct Recovery = 105% Analysis Date = 05/22/14 Pct Recovery = 105% Analysis Date = 05/17/14 Pct Recovery = 105% Analysis Date = 05/17/14 Pct Recovery = 105% Analysis Date = 05/12/14 Pct Recovery = 105% Analysis Date = 05/12/14 Pct Recovery = 105% Analysis Date = 05/07/14 Pct Recovery = 105% Analysis Date = 05/07/14 Pct Recovery = 105% Analysis Date = 05/03/14 Pct Recovery = 105% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
ETHYL TERT-BUTYL ETHER

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 47 101% 15% 100% 15%
Total 47 101% 15% 100% 15%

Sample Statistics
ETHYL TERT-BUTYL ETHER

Characteristic N % % Basis
Plotted 47 100% Spiked
Estimated Values 2 4% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 47 .  
False Negatives 0 0% 0 out of 47
Not Spiked 26 .  
False Positives 0 0% 0 out of 26

BQS OBSP Determination:
HEXACHLOROBUTADIENE
METHOD: 4440 , TESTIDCODE: 39702GCM66
Open Data Set

Analysis Date = 12/16/16 SpikeMix = NSI 041816AVOC: 40 µl & ChemService 5082900: 40 µl Pct Recovery = 100% Analysis Date = 07/14/16 SpikeMix = Accu 216041125: 40 µl & NSI 041816AVOC: 40 µl Pct Recovery = 105% Analysis Date = 12/12/16 SpikeMix = Accu 216041125: 40 µl & Crescent 03FF058: 40 µl Pct Recovery = 87% Analysis Date = 08/04/16 SpikeMix = Crescent 03FF058: 40 µl & Supelco LC20141V: 40 µl Pct Recovery = 93% Analysis Date = 08/26/16 SpikeMix = NSI 041816AVOC: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 102% Analysis Date = 11/21/16 SpikeMix = Crescent 03FF058: 25 µl & Supelco LC20141V: 25 µl Pct Recovery = 86% Analysis Date = 06/30/16 SpikeMix = Crescent 03FF058: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 90% Analysis Date = 06/21/16 SpikeMix = Phenova B20160319: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 79% Analysis Date = 05/24/16 SpikeMix = Accu 216041125: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 79% Analysis Date = 04/09/15 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 94% Analysis Date = 08/19/14 SpikeMix = Spex Organics C1140417015: 20 µl & Accu 214031115: 20 µl Pct Recovery = 86% Analysis Date = 07/01/14 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 86% Analysis Date = 05/01/14 SpikeMix = Accu 214031115: 20 µl & NSI 032614: 20 µl Pct Recovery = 82% Analysis Date = 03/19/15 SpikeMix = Spex Organics C1140417015: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 88% Analysis Date = 12/17/14 SpikeMix = Supelco LC06438: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 84% Analysis Date = 11/14/14 SpikeMix = Crescent 03DD004: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 79% Analysis Date = 06/10/14 SpikeMix = Crescent 03DD004: 20 µl & NSI 032614: 20 µl Pct Recovery = 76% Analysis Date = 08/15/15 SpikeMix = Supelco LC13545: 25 µl & Crescent 04EE008: 25 µl Pct Recovery = 95% Analysis Date = 06/16/15 SpikeMix = ERA 0406-15-03: 25 µl & Supelco LC13545: 25 µl Pct Recovery = 82% Analysis Date = 10/13/16 SpikeMix = Accu 216041125: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 93% Analysis Date = 10/13/16 SpikeMix = NSI 041816AVOC: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 96% Analysis Date = 07/29/16 SpikeMix = Phenova B20160319: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 93% Analysis Date = 06/10/16 SpikeMix = NSI 041816AVOC: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 87% Analysis Date = 09/28/16 SpikeMix = Crescent 03FF058: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 73% Analysis Date = 09/08/16 SpikeMix = Phenova B20160319: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 85% Analysis Date = 08/20/16 SpikeMix = Accu 216041125: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 86% Analysis Date = 04/02/16 SpikeMix = Supelco LC13545: 15 µl & Accu 215041380: 15 µl Pct Recovery = 86% Analysis Date = 12/18/15 SpikeMix = Supelco LC13545: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 71% Analysis Date = 04/26/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 83% Analysis Date = 02/05/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 79% Analysis Date = 11/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 73% Analysis Date = 10/16/15 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 79% Analysis Date = 05/09/15 SpikeMix = Spex Organics EN150428007: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 89% Analysis Date = 01/13/15 SpikeMix = Accu 214031115: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 76% Analysis Date = 09/09/14 SpikeMix = Accu 214031115: 10 µl & NSI 032614: 10 µl Pct Recovery = 92% Analysis Date = 07/23/14 SpikeMix = Spex Organics C1140417015: 10 µl & Accu 214031115: 10 µl Pct Recovery = 98% Analysis Date = 06/18/14 SpikeMix = Supelco LC06438: 10 µl & Accu 214031115: 10 µl Pct Recovery = 89% Analysis Date = 11/06/14 SpikeMix = Spex Organics C1140417015: 10 µl & Crescent 03DD004: 10 µl Pct Recovery = 79% Analysis Date = 10/04/14 SpikeMix = Crescent 03DD004: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 97% Analysis Date = 07/29/14 SpikeMix = Crescent 03DD004: 10 µl & NSI 032614: 10 µl Pct Recovery = 90% Analysis Date = 05/03/14 SpikeMix = Crescent 03DD004: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 85% Analysis Date = 05/13/16 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 95% Analysis Date = 03/17/16 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 75% Analysis Date = 12/10/15 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 77% Analysis Date = 06/27/15 SpikeMix = ERA 0406-15-03: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 86% Analysis Date = 05/09/15 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 84% Analysis Date = 02/18/16 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 88% Analysis Date = 11/12/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 79% Analysis Date = 09/03/15 SpikeMix = NSI 050515AVOC: 10 µl & Spex Organics EN150428007: 10 µl Pct Recovery = 86% Analysis Date = 05/21/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 90% Analysis Date = 12/15/16 Pct Recovery = 93% Analysis Date = 12/11/16 Pct Recovery = 93% Analysis Date = 12/11/16 Pct Recovery = 93% Analysis Date = 12/06/16 Pct Recovery = 93% Analysis Date = 12/06/16 Pct Recovery = 93% Analysis Date = 12/01/16 Pct Recovery = 93% Analysis Date = 12/01/16 Pct Recovery = 93% Analysis Date = 11/26/16 Pct Recovery = 93% Analysis Date = 11/26/16 Pct Recovery = 93% Analysis Date = 11/21/16 Pct Recovery = 93% Analysis Date = 11/21/16 Pct Recovery = 93% Analysis Date = 11/17/16 Pct Recovery = 92% Analysis Date = 11/17/16 Pct Recovery = 92% Analysis Date = 11/12/16 Pct Recovery = 92% Analysis Date = 11/12/16 Pct Recovery = 92% Analysis Date = 11/07/16 Pct Recovery = 92% Analysis Date = 11/07/16 Pct Recovery = 92% Analysis Date = 11/02/16 Pct Recovery = 92% Analysis Date = 11/02/16 Pct Recovery = 92% Analysis Date = 10/28/16 Pct Recovery = 92% Analysis Date = 10/28/16 Pct Recovery = 92% Analysis Date = 10/24/16 Pct Recovery = 92% Analysis Date = 10/24/16 Pct Recovery = 92% Analysis Date = 10/19/16 Pct Recovery = 91% Analysis Date = 10/19/16 Pct Recovery = 91% Analysis Date = 10/14/16 Pct Recovery = 91% Analysis Date = 10/14/16 Pct Recovery = 91% Analysis Date = 10/09/16 Pct Recovery = 91% Analysis Date = 10/09/16 Pct Recovery = 91% Analysis Date = 10/04/16 Pct Recovery = 91% Analysis Date = 10/04/16 Pct Recovery = 91% Analysis Date = 09/30/16 Pct Recovery = 91% Analysis Date = 09/30/16 Pct Recovery = 91% Analysis Date = 09/25/16 Pct Recovery = 91% Analysis Date = 09/25/16 Pct Recovery = 91% Analysis Date = 09/20/16 Pct Recovery = 90% Analysis Date = 09/20/16 Pct Recovery = 90% Analysis Date = 09/15/16 Pct Recovery = 90% Analysis Date = 09/15/16 Pct Recovery = 90% Analysis Date = 09/10/16 Pct Recovery = 90% Analysis Date = 09/10/16 Pct Recovery = 90% Analysis Date = 09/06/16 Pct Recovery = 90% Analysis Date = 09/06/16 Pct Recovery = 90% Analysis Date = 09/01/16 Pct Recovery = 90% Analysis Date = 09/01/16 Pct Recovery = 90% Analysis Date = 08/27/16 Pct Recovery = 89% Analysis Date = 08/27/16 Pct Recovery = 89% Analysis Date = 08/22/16 Pct Recovery = 89% Analysis Date = 08/22/16 Pct Recovery = 89% Analysis Date = 08/17/16 Pct Recovery = 89% Analysis Date = 08/17/16 Pct Recovery = 89% Analysis Date = 08/13/16 Pct Recovery = 89% Analysis Date = 08/13/16 Pct Recovery = 89% Analysis Date = 08/08/16 Pct Recovery = 89% Analysis Date = 08/08/16 Pct Recovery = 89% Analysis Date = 08/03/16 Pct Recovery = 89% Analysis Date = 08/03/16 Pct Recovery = 89% Analysis Date = 07/29/16 Pct Recovery = 88% Analysis Date = 07/29/16 Pct Recovery = 88% Analysis Date = 07/24/16 Pct Recovery = 88% Analysis Date = 07/24/16 Pct Recovery = 88% Analysis Date = 07/20/16 Pct Recovery = 88% Analysis Date = 07/20/16 Pct Recovery = 88% Analysis Date = 07/15/16 Pct Recovery = 88% Analysis Date = 07/15/16 Pct Recovery = 88% Analysis Date = 07/10/16 Pct Recovery = 88% Analysis Date = 07/10/16 Pct Recovery = 88% Analysis Date = 07/05/16 Pct Recovery = 87% Analysis Date = 07/05/16 Pct Recovery = 87% Analysis Date = 06/30/16 Pct Recovery = 87% Analysis Date = 06/30/16 Pct Recovery = 87% Analysis Date = 06/26/16 Pct Recovery = 87% Analysis Date = 06/26/16 Pct Recovery = 87% Analysis Date = 06/21/16 Pct Recovery = 87% Analysis Date = 06/21/16 Pct Recovery = 87% Analysis Date = 06/16/16 Pct Recovery = 87% Analysis Date = 06/16/16 Pct Recovery = 87% Analysis Date = 06/11/16 Pct Recovery = 87% Analysis Date = 06/11/16 Pct Recovery = 87% Analysis Date = 06/06/16 Pct Recovery = 86% Analysis Date = 06/06/16 Pct Recovery = 86% Analysis Date = 06/02/16 Pct Recovery = 86% Analysis Date = 06/02/16 Pct Recovery = 86% Analysis Date = 05/28/16 Pct Recovery = 86% Analysis Date = 05/28/16 Pct Recovery = 86% Analysis Date = 05/23/16 Pct Recovery = 86% Analysis Date = 05/23/16 Pct Recovery = 86% Analysis Date = 05/18/16 Pct Recovery = 86% Analysis Date = 05/18/16 Pct Recovery = 86% Analysis Date = 05/13/16 Pct Recovery = 85% Analysis Date = 05/13/16 Pct Recovery = 85% Analysis Date = 05/09/16 Pct Recovery = 85% Analysis Date = 05/09/16 Pct Recovery = 85% Analysis Date = 05/04/16 Pct Recovery = 85% Analysis Date = 05/04/16 Pct Recovery = 85% Analysis Date = 04/29/16 Pct Recovery = 85% Analysis Date = 04/29/16 Pct Recovery = 85% Analysis Date = 04/24/16 Pct Recovery = 85% Analysis Date = 04/24/16 Pct Recovery = 85% Analysis Date = 04/19/16 Pct Recovery = 85% Analysis Date = 04/19/16 Pct Recovery = 85% Analysis Date = 04/15/16 Pct Recovery = 84% Analysis Date = 04/15/16 Pct Recovery = 84% Analysis Date = 04/10/16 Pct Recovery = 84% Analysis Date = 04/10/16 Pct Recovery = 84% Analysis Date = 04/05/16 Pct Recovery = 84% Analysis Date = 04/05/16 Pct Recovery = 84% Analysis Date = 03/31/16 Pct Recovery = 84% Analysis Date = 03/31/16 Pct Recovery = 84% Analysis Date = 03/26/16 Pct Recovery = 84% Analysis Date = 03/26/16 Pct Recovery = 84% Analysis Date = 03/22/16 Pct Recovery = 84% Analysis Date = 03/22/16 Pct Recovery = 84% Analysis Date = 03/17/16 Pct Recovery = 83% Analysis Date = 03/17/16 Pct Recovery = 83% Analysis Date = 03/12/16 Pct Recovery = 83% Analysis Date = 03/12/16 Pct Recovery = 83% Analysis Date = 03/07/16 Pct Recovery = 83% Analysis Date = 03/07/16 Pct Recovery = 83% Analysis Date = 03/02/16 Pct Recovery = 83% Analysis Date = 03/02/16 Pct Recovery = 83% Analysis Date = 02/27/16 Pct Recovery = 83% Analysis Date = 02/27/16 Pct Recovery = 83% Analysis Date = 02/22/16 Pct Recovery = 83% Analysis Date = 02/22/16 Pct Recovery = 83% Analysis Date = 02/17/16 Pct Recovery = 83% Analysis Date = 02/17/16 Pct Recovery = 83% Analysis Date = 02/12/16 Pct Recovery = 82% Analysis Date = 02/12/16 Pct Recovery = 82% Analysis Date = 02/07/16 Pct Recovery = 82% Analysis Date = 02/07/16 Pct Recovery = 82% Analysis Date = 02/03/16 Pct Recovery = 82% Analysis Date = 02/03/16 Pct Recovery = 82% Analysis Date = 01/29/16 Pct Recovery = 82% Analysis Date = 01/29/16 Pct Recovery = 82% Analysis Date = 01/24/16 Pct Recovery = 82% Analysis Date = 01/24/16 Pct Recovery = 82% Analysis Date = 01/19/16 Pct Recovery = 82% Analysis Date = 01/19/16 Pct Recovery = 82% Analysis Date = 01/14/16 Pct Recovery = 82% Analysis Date = 01/14/16 Pct Recovery = 82% Analysis Date = 01/10/16 Pct Recovery = 82% Analysis Date = 01/10/16 Pct Recovery = 82% Analysis Date = 01/05/16 Pct Recovery = 82% Analysis Date = 01/05/16 Pct Recovery = 82% Analysis Date = 12/31/15 Pct Recovery = 82% Analysis Date = 12/31/15 Pct Recovery = 82% Analysis Date = 12/26/15 Pct Recovery = 82% Analysis Date = 12/26/15 Pct Recovery = 82% Analysis Date = 12/21/15 Pct Recovery = 82% Analysis Date = 12/21/15 Pct Recovery = 82% Analysis Date = 12/17/15 Pct Recovery = 82% Analysis Date = 12/17/15 Pct Recovery = 82% Analysis Date = 12/12/15 Pct Recovery = 82% Analysis Date = 12/12/15 Pct Recovery = 82% Analysis Date = 12/07/15 Pct Recovery = 82% Analysis Date = 12/07/15 Pct Recovery = 82% Analysis Date = 12/02/15 Pct Recovery = 82% Analysis Date = 12/02/15 Pct Recovery = 82% Analysis Date = 11/27/15 Pct Recovery = 83% Analysis Date = 11/27/15 Pct Recovery = 83% Analysis Date = 11/23/15 Pct Recovery = 83% Analysis Date = 11/23/15 Pct Recovery = 83% Analysis Date = 11/18/15 Pct Recovery = 83% Analysis Date = 11/18/15 Pct Recovery = 83% Analysis Date = 11/13/15 Pct Recovery = 83% Analysis Date = 11/13/15 Pct Recovery = 83% Analysis Date = 11/08/15 Pct Recovery = 83% Analysis Date = 11/08/15 Pct Recovery = 83% Analysis Date = 11/03/15 Pct Recovery = 83% Analysis Date = 11/03/15 Pct Recovery = 83% Analysis Date = 10/30/15 Pct Recovery = 83% Analysis Date = 10/30/15 Pct Recovery = 83% Analysis Date = 10/25/15 Pct Recovery = 83% Analysis Date = 10/25/15 Pct Recovery = 83% Analysis Date = 10/20/15 Pct Recovery = 83% Analysis Date = 10/20/15 Pct Recovery = 83% Analysis Date = 10/15/15 Pct Recovery = 83% Analysis Date = 10/15/15 Pct Recovery = 83% Analysis Date = 10/10/15 Pct Recovery = 83% Analysis Date = 10/10/15 Pct Recovery = 83% Analysis Date = 10/06/15 Pct Recovery = 83% Analysis Date = 10/06/15 Pct Recovery = 83% Analysis Date = 10/01/15 Pct Recovery = 83% Analysis Date = 10/01/15 Pct Recovery = 83% Analysis Date = 09/26/15 Pct Recovery = 83% Analysis Date = 09/26/15 Pct Recovery = 83% Analysis Date = 09/21/15 Pct Recovery = 83% Analysis Date = 09/21/15 Pct Recovery = 83% Analysis Date = 09/16/15 Pct Recovery = 83% Analysis Date = 09/16/15 Pct Recovery = 83% Analysis Date = 09/12/15 Pct Recovery = 83% Analysis Date = 09/12/15 Pct Recovery = 83% Analysis Date = 09/07/15 Pct Recovery = 83% Analysis Date = 09/07/15 Pct Recovery = 83% Analysis Date = 09/02/15 Pct Recovery = 83% Analysis Date = 09/02/15 Pct Recovery = 83% Analysis Date = 08/28/15 Pct Recovery = 83% Analysis Date = 08/28/15 Pct Recovery = 83% Analysis Date = 08/23/15 Pct Recovery = 83% Analysis Date = 08/23/15 Pct Recovery = 83% Analysis Date = 08/19/15 Pct Recovery = 83% Analysis Date = 08/19/15 Pct Recovery = 83% Analysis Date = 08/14/15 Pct Recovery = 84% Analysis Date = 08/14/15 Pct Recovery = 84% Analysis Date = 08/09/15 Pct Recovery = 84% Analysis Date = 08/09/15 Pct Recovery = 84% Analysis Date = 08/04/15 Pct Recovery = 84% Analysis Date = 08/04/15 Pct Recovery = 84% Analysis Date = 07/30/15 Pct Recovery = 84% Analysis Date = 07/30/15 Pct Recovery = 84% Analysis Date = 07/26/15 Pct Recovery = 84% Analysis Date = 07/26/15 Pct Recovery = 84% Analysis Date = 07/21/15 Pct Recovery = 84% Analysis Date = 07/21/15 Pct Recovery = 84% Analysis Date = 07/16/15 Pct Recovery = 84% Analysis Date = 07/16/15 Pct Recovery = 84% Analysis Date = 07/11/15 Pct Recovery = 84% Analysis Date = 07/11/15 Pct Recovery = 84% Analysis Date = 07/06/15 Pct Recovery = 84% Analysis Date = 07/06/15 Pct Recovery = 84% Analysis Date = 07/02/15 Pct Recovery = 84% Analysis Date = 07/02/15 Pct Recovery = 84% Analysis Date = 06/27/15 Pct Recovery = 84% Analysis Date = 06/27/15 Pct Recovery = 84% Analysis Date = 06/22/15 Pct Recovery = 84% Analysis Date = 06/22/15 Pct Recovery = 84% Analysis Date = 06/17/15 Pct Recovery = 84% Analysis Date = 06/17/15 Pct Recovery = 84% Analysis Date = 06/12/15 Pct Recovery = 84% Analysis Date = 06/12/15 Pct Recovery = 84% Analysis Date = 06/08/15 Pct Recovery = 84% Analysis Date = 06/08/15 Pct Recovery = 84% Analysis Date = 06/03/15 Pct Recovery = 84% Analysis Date = 06/03/15 Pct Recovery = 84% Analysis Date = 05/29/15 Pct Recovery = 84% Analysis Date = 05/29/15 Pct Recovery = 84% Analysis Date = 05/24/15 Pct Recovery = 85% Analysis Date = 05/24/15 Pct Recovery = 85% Analysis Date = 05/19/15 Pct Recovery = 85% Analysis Date = 05/19/15 Pct Recovery = 85% Analysis Date = 05/15/15 Pct Recovery = 85% Analysis Date = 05/15/15 Pct Recovery = 85% Analysis Date = 05/10/15 Pct Recovery = 85% Analysis Date = 05/10/15 Pct Recovery = 85% Analysis Date = 05/05/15 Pct Recovery = 85% Analysis Date = 05/05/15 Pct Recovery = 85% Analysis Date = 04/30/15 Pct Recovery = 85% Analysis Date = 04/30/15 Pct Recovery = 85% Analysis Date = 04/25/15 Pct Recovery = 85% Analysis Date = 04/25/15 Pct Recovery = 85% Analysis Date = 04/21/15 Pct Recovery = 85% Analysis Date = 04/21/15 Pct Recovery = 85% Analysis Date = 04/16/15 Pct Recovery = 85% Analysis Date = 04/16/15 Pct Recovery = 85% Analysis Date = 04/11/15 Pct Recovery = 85% Analysis Date = 04/11/15 Pct Recovery = 85% Analysis Date = 04/06/15 Pct Recovery = 85% Analysis Date = 04/06/15 Pct Recovery = 85% Analysis Date = 04/01/15 Pct Recovery = 85% Analysis Date = 04/01/15 Pct Recovery = 85% Analysis Date = 03/28/15 Pct Recovery = 85% Analysis Date = 03/28/15 Pct Recovery = 85% Analysis Date = 03/23/15 Pct Recovery = 85% Analysis Date = 03/23/15 Pct Recovery = 85% Analysis Date = 03/18/15 Pct Recovery = 85% Analysis Date = 03/18/15 Pct Recovery = 85% Analysis Date = 03/13/15 Pct Recovery = 85% Analysis Date = 03/13/15 Pct Recovery = 85% Analysis Date = 03/08/15 Pct Recovery = 85% Analysis Date = 03/08/15 Pct Recovery = 85% Analysis Date = 03/04/15 Pct Recovery = 85% Analysis Date = 03/04/15 Pct Recovery = 85% Analysis Date = 02/27/15 Pct Recovery = 85% Analysis Date = 02/27/15 Pct Recovery = 85% Analysis Date = 02/22/15 Pct Recovery = 86% Analysis Date = 02/22/15 Pct Recovery = 86% Analysis Date = 02/17/15 Pct Recovery = 86% Analysis Date = 02/17/15 Pct Recovery = 86% Analysis Date = 02/12/15 Pct Recovery = 86% Analysis Date = 02/12/15 Pct Recovery = 86% Analysis Date = 02/08/15 Pct Recovery = 86% Analysis Date = 02/08/15 Pct Recovery = 86% Analysis Date = 02/03/15 Pct Recovery = 86% Analysis Date = 02/03/15 Pct Recovery = 86% Analysis Date = 01/29/15 Pct Recovery = 86% Analysis Date = 01/29/15 Pct Recovery = 86% Analysis Date = 01/24/15 Pct Recovery = 86% Analysis Date = 01/24/15 Pct Recovery = 86% Analysis Date = 01/19/15 Pct Recovery = 86% Analysis Date = 01/19/15 Pct Recovery = 86% Analysis Date = 01/15/15 Pct Recovery = 86% Analysis Date = 01/15/15 Pct Recovery = 86% Analysis Date = 01/10/15 Pct Recovery = 86% Analysis Date = 01/10/15 Pct Recovery = 86% Analysis Date = 01/05/15 Pct Recovery = 86% Analysis Date = 01/05/15 Pct Recovery = 86% Analysis Date = 12/31/14 Pct Recovery = 86% Analysis Date = 12/31/14 Pct Recovery = 86% Analysis Date = 12/26/14 Pct Recovery = 86% Analysis Date = 12/26/14 Pct Recovery = 86% Analysis Date = 12/22/14 Pct Recovery = 86% Analysis Date = 12/22/14 Pct Recovery = 86% Analysis Date = 12/17/14 Pct Recovery = 86% Analysis Date = 12/17/14 Pct Recovery = 86% Analysis Date = 12/12/14 Pct Recovery = 86% Analysis Date = 12/12/14 Pct Recovery = 86% Analysis Date = 12/07/14 Pct Recovery = 86% Analysis Date = 12/07/14 Pct Recovery = 86% Analysis Date = 12/02/14 Pct Recovery = 86% Analysis Date = 12/02/14 Pct Recovery = 86% Analysis Date = 11/28/14 Pct Recovery = 86% Analysis Date = 11/28/14 Pct Recovery = 86% Analysis Date = 11/23/14 Pct Recovery = 86% Analysis Date = 11/23/14 Pct Recovery = 86% Analysis Date = 11/18/14 Pct Recovery = 86% Analysis Date = 11/18/14 Pct Recovery = 86% Analysis Date = 11/13/14 Pct Recovery = 86% Analysis Date = 11/13/14 Pct Recovery = 86% Analysis Date = 11/08/14 Pct Recovery = 86% Analysis Date = 11/08/14 Pct Recovery = 86% Analysis Date = 11/04/14 Pct Recovery = 86% Analysis Date = 11/04/14 Pct Recovery = 86% Analysis Date = 10/30/14 Pct Recovery = 86% Analysis Date = 10/30/14 Pct Recovery = 86% Analysis Date = 10/25/14 Pct Recovery = 86% Analysis Date = 10/25/14 Pct Recovery = 86% Analysis Date = 10/20/14 Pct Recovery = 86% Analysis Date = 10/20/14 Pct Recovery = 86% Analysis Date = 10/15/14 Pct Recovery = 86% Analysis Date = 10/15/14 Pct Recovery = 86% Analysis Date = 10/11/14 Pct Recovery = 86% Analysis Date = 10/11/14 Pct Recovery = 86% Analysis Date = 10/06/14 Pct Recovery = 86% Analysis Date = 10/06/14 Pct Recovery = 86% Analysis Date = 10/01/14 Pct Recovery = 86% Analysis Date = 10/01/14 Pct Recovery = 86% Analysis Date = 09/26/14 Pct Recovery = 86% Analysis Date = 09/26/14 Pct Recovery = 86% Analysis Date = 09/21/14 Pct Recovery = 86% Analysis Date = 09/21/14 Pct Recovery = 86% Analysis Date = 09/17/14 Pct Recovery = 86% Analysis Date = 09/17/14 Pct Recovery = 86% Analysis Date = 09/12/14 Pct Recovery = 86% Analysis Date = 09/12/14 Pct Recovery = 86% Analysis Date = 09/07/14 Pct Recovery = 86% Analysis Date = 09/07/14 Pct Recovery = 86% Analysis Date = 09/02/14 Pct Recovery = 86% Analysis Date = 09/02/14 Pct Recovery = 86% Analysis Date = 08/28/14 Pct Recovery = 86% Analysis Date = 08/28/14 Pct Recovery = 86% Analysis Date = 08/24/14 Pct Recovery = 86% Analysis Date = 08/24/14 Pct Recovery = 86% Analysis Date = 08/19/14 Pct Recovery = 86% Analysis Date = 08/19/14 Pct Recovery = 86% Analysis Date = 08/14/14 Pct Recovery = 86% Analysis Date = 08/14/14 Pct Recovery = 86% Analysis Date = 08/09/14 Pct Recovery = 86% Analysis Date = 08/09/14 Pct Recovery = 86% Analysis Date = 08/04/14 Pct Recovery = 86% Analysis Date = 08/04/14 Pct Recovery = 86% Analysis Date = 07/31/14 Pct Recovery = 86% Analysis Date = 07/31/14 Pct Recovery = 86% Analysis Date = 07/26/14 Pct Recovery = 86% Analysis Date = 07/26/14 Pct Recovery = 86% Analysis Date = 07/21/14 Pct Recovery = 86% Analysis Date = 07/21/14 Pct Recovery = 86% Analysis Date = 07/16/14 Pct Recovery = 86% Analysis Date = 07/16/14 Pct Recovery = 86% Analysis Date = 07/11/14 Pct Recovery = 86% Analysis Date = 07/11/14 Pct Recovery = 86% Analysis Date = 07/07/14 Pct Recovery = 86% Analysis Date = 07/07/14 Pct Recovery = 86% Analysis Date = 07/02/14 Pct Recovery = 86% Analysis Date = 07/02/14 Pct Recovery = 86% Analysis Date = 06/27/14 Pct Recovery = 86% Analysis Date = 06/27/14 Pct Recovery = 86% Analysis Date = 06/22/14 Pct Recovery = 86% Analysis Date = 06/22/14 Pct Recovery = 86% Analysis Date = 06/17/14 Pct Recovery = 86% Analysis Date = 06/17/14 Pct Recovery = 86% Analysis Date = 06/13/14 Pct Recovery = 86% Analysis Date = 06/13/14 Pct Recovery = 86% Analysis Date = 06/08/14 Pct Recovery = 86% Analysis Date = 06/08/14 Pct Recovery = 86% Analysis Date = 06/03/14 Pct Recovery = 86% Analysis Date = 06/03/14 Pct Recovery = 86% Analysis Date = 05/29/14 Pct Recovery = 86% Analysis Date = 05/29/14 Pct Recovery = 86% Analysis Date = 05/24/14 Pct Recovery = 86% Analysis Date = 05/24/14 Pct Recovery = 86% Analysis Date = 05/20/14 Pct Recovery = 86% Analysis Date = 05/20/14 Pct Recovery = 86% Analysis Date = 05/15/14 Pct Recovery = 86% Analysis Date = 05/15/14 Pct Recovery = 86% Analysis Date = 05/10/14 Pct Recovery = 86% Analysis Date = 05/10/14 Pct Recovery = 86% Analysis Date = 05/05/14 Pct Recovery = 86% Analysis Date = 05/05/14 Pct Recovery = 86% Analysis Date = 05/01/14 Pct Recovery = 86% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
HEXACHLOROBUTADIENE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 50 86% 8% 86% 10%
Total 50 86% 8% 86% 10%

Sample Statistics
HEXACHLOROBUTADIENE

Characteristic N % % Basis
Plotted 50 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 50 .  
False Negatives 0 0% 0 out of 50
Not Spiked 23 .  
False Positives 0 0% 0 out of 23

BQS OBSP Determination:
HEXACHLOROETHANE
METHOD: 4440 , TESTIDCODE: 34396GCM66
Open Data Set

Analysis Date = 12/12/16 SpikeMix = Accu 216041125: 40 µl & Crescent 03FF058: 40 µl Pct Recovery = 90% Analysis Date = 07/20/16 SpikeMix = Supelco LC20141V: 40 µl & Accu 216041125: 40 µl Pct Recovery = 97% Analysis Date = 07/14/16 SpikeMix = Accu 216041125: 40 µl & NSI 041816AVOC: 40 µl Pct Recovery = 91% Analysis Date = 08/12/16 SpikeMix = ChemService 5082900: 25 µl & Phenova B20160319: 25 µl Pct Recovery = 80% Analysis Date = 06/21/16 SpikeMix = Phenova B20160319: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 84% Analysis Date = 09/08/16 SpikeMix = Supelco LC20141V: 25 µl & Accu 216041125: 25 µl Pct Recovery = 74% Analysis Date = 05/24/16 SpikeMix = Accu 216041125: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 85% Analysis Date = 03/06/15 SpikeMix = ERA 0227-14-06.1A: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 85% Analysis Date = 12/17/14 SpikeMix = Supelco LC06438: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 83% Analysis Date = 09/21/14 SpikeMix = Supelco LC06438: 20 µl Pct Recovery = 95% Analysis Date = 06/10/14 SpikeMix = NSI 032614: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 90% Analysis Date = 03/19/15 SpikeMix = Spex Organics C1140417015: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 89% Analysis Date = 11/22/14 SpikeMix = NSI 032614: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 97% Analysis Date = 08/19/14 SpikeMix = Spex Organics C1140417015: 20 µl & Accu 214031115: 20 µl Pct Recovery = 98% Analysis Date = 08/16/14 SpikeMix = ERA 0227-14-06.1A: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 103% Analysis Date = 08/15/15 SpikeMix = Supelco LC13545: 25 µl & Crescent 04EE008: 25 µl Pct Recovery = 109% Analysis Date = 06/16/15 SpikeMix = ERA 0406-15-03: 25 µl & Supelco LC13545: 25 µl Pct Recovery = 83% Analysis Date = 11/29/16 SpikeMix = ChemService 5082900: 15 µl & Phenova B20160319: 15 µl Pct Recovery = 80% Analysis Date = 09/08/16 SpikeMix = Phenova B20160319: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 92% Analysis Date = 07/29/16 SpikeMix = Phenova B20160319: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 116% Analysis Date = 05/27/16 SpikeMix = Phenova B20160319: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 93% Analysis Date = 10/13/16 SpikeMix = Accu 216041125: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 80% Analysis Date = 08/20/16 SpikeMix = Accu 216041125: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 86% Analysis Date = 06/30/16 SpikeMix = ChemService 5082900: 15 µl & Accu 216041125: 15 µl Pct Recovery = 63% Analysis Date = 04/02/16 SpikeMix = Supelco LC13545: 15 µl & Accu 215041380: 15 µl Pct Recovery = 100% Analysis Date = 12/18/15 SpikeMix = Supelco LC13545: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 92% Analysis Date = 04/26/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 113% Analysis Date = 02/05/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 84% Analysis Date = 11/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 87% Analysis Date = 10/16/15 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 91% Analysis Date = 05/09/15 SpikeMix = Spex Organics EN150428007: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 88% Analysis Date = 10/21/14 SpikeMix = ERA 0227-14-06.1A: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 88% Analysis Date = 06/18/14 SpikeMix = Supelco LC06438: 10 µl & Accu 214031115: 10 µl Pct Recovery = 103% Analysis Date = 05/30/14 SpikeMix = NSI 032614: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 92% Analysis Date = 05/03/14 SpikeMix = Crescent 03DD004: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 93% Analysis Date = 11/06/14 SpikeMix = Spex Organics C1140417015: 10 µl & Crescent 03DD004: 10 µl Pct Recovery = 90% Analysis Date = 09/09/14 SpikeMix = NSI 032614: 10 µl & Spex Organics C1140417015: 10 µl Pct Recovery = 95% Analysis Date = 07/23/14 SpikeMix = Spex Organics C1140417015: 10 µl & Accu 214031115: 10 µl Pct Recovery = 105% Analysis Date = 07/11/14 SpikeMix = Spex Organics C1140417015: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 92% Analysis Date = 05/13/16 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 113% Analysis Date = 03/17/16 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 113% Analysis Date = 12/10/15 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 103% Analysis Date = 06/27/15 SpikeMix = ERA 0406-15-03: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 96% Analysis Date = 05/09/15 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 91% Analysis Date = 02/18/16 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 117% Analysis Date = 11/12/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 95% Analysis Date = 09/03/15 SpikeMix = NSI 050515AVOC: 10 µl & Spex Organics EN150428007: 10 µl Pct Recovery = 116% Analysis Date = 05/21/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 84% Analysis Date = 12/12/16 Pct Recovery = 82% Analysis Date = 12/07/16 Pct Recovery = 82% Analysis Date = 12/07/16 Pct Recovery = 82% Analysis Date = 12/02/16 Pct Recovery = 83% Analysis Date = 12/02/16 Pct Recovery = 83% Analysis Date = 11/27/16 Pct Recovery = 83% Analysis Date = 11/27/16 Pct Recovery = 83% Analysis Date = 11/22/16 Pct Recovery = 83% Analysis Date = 11/22/16 Pct Recovery = 83% Analysis Date = 11/18/16 Pct Recovery = 84% Analysis Date = 11/18/16 Pct Recovery = 84% Analysis Date = 11/13/16 Pct Recovery = 84% Analysis Date = 11/13/16 Pct Recovery = 84% Analysis Date = 11/08/16 Pct Recovery = 84% Analysis Date = 11/08/16 Pct Recovery = 84% Analysis Date = 11/03/16 Pct Recovery = 84% Analysis Date = 11/03/16 Pct Recovery = 84% Analysis Date = 10/30/16 Pct Recovery = 85% Analysis Date = 10/30/16 Pct Recovery = 85% Analysis Date = 10/25/16 Pct Recovery = 85% Analysis Date = 10/25/16 Pct Recovery = 85% Analysis Date = 10/20/16 Pct Recovery = 85% Analysis Date = 10/20/16 Pct Recovery = 85% Analysis Date = 10/15/16 Pct Recovery = 86% Analysis Date = 10/15/16 Pct Recovery = 86% Analysis Date = 10/10/16 Pct Recovery = 86% Analysis Date = 10/10/16 Pct Recovery = 86% Analysis Date = 10/06/16 Pct Recovery = 86% Analysis Date = 10/06/16 Pct Recovery = 86% Analysis Date = 10/01/16 Pct Recovery = 86% Analysis Date = 10/01/16 Pct Recovery = 86% Analysis Date = 09/26/16 Pct Recovery = 87% Analysis Date = 09/26/16 Pct Recovery = 87% Analysis Date = 09/21/16 Pct Recovery = 87% Analysis Date = 09/21/16 Pct Recovery = 87% Analysis Date = 09/17/16 Pct Recovery = 87% Analysis Date = 09/17/16 Pct Recovery = 87% Analysis Date = 09/12/16 Pct Recovery = 88% Analysis Date = 09/12/16 Pct Recovery = 88% Analysis Date = 09/07/16 Pct Recovery = 88% Analysis Date = 09/07/16 Pct Recovery = 88% Analysis Date = 09/02/16 Pct Recovery = 88% Analysis Date = 09/02/16 Pct Recovery = 88% Analysis Date = 08/29/16 Pct Recovery = 88% Analysis Date = 08/29/16 Pct Recovery = 88% Analysis Date = 08/24/16 Pct Recovery = 89% Analysis Date = 08/24/16 Pct Recovery = 89% Analysis Date = 08/19/16 Pct Recovery = 89% Analysis Date = 08/19/16 Pct Recovery = 89% Analysis Date = 08/14/16 Pct Recovery = 89% Analysis Date = 08/14/16 Pct Recovery = 89% Analysis Date = 08/09/16 Pct Recovery = 89% Analysis Date = 08/09/16 Pct Recovery = 89% Analysis Date = 08/05/16 Pct Recovery = 90% Analysis Date = 08/05/16 Pct Recovery = 90% Analysis Date = 07/31/16 Pct Recovery = 90% Analysis Date = 07/31/16 Pct Recovery = 90% Analysis Date = 07/26/16 Pct Recovery = 90% Analysis Date = 07/26/16 Pct Recovery = 90% Analysis Date = 07/21/16 Pct Recovery = 91% Analysis Date = 07/21/16 Pct Recovery = 91% Analysis Date = 07/17/16 Pct Recovery = 91% Analysis Date = 07/17/16 Pct Recovery = 91% Analysis Date = 07/12/16 Pct Recovery = 91% Analysis Date = 07/12/16 Pct Recovery = 91% Analysis Date = 07/07/16 Pct Recovery = 91% Analysis Date = 07/07/16 Pct Recovery = 91% Analysis Date = 07/02/16 Pct Recovery = 92% Analysis Date = 07/02/16 Pct Recovery = 92% Analysis Date = 06/28/16 Pct Recovery = 92% Analysis Date = 06/28/16 Pct Recovery = 92% Analysis Date = 06/23/16 Pct Recovery = 92% Analysis Date = 06/23/16 Pct Recovery = 92% Analysis Date = 06/18/16 Pct Recovery = 92% Analysis Date = 06/18/16 Pct Recovery = 92% Analysis Date = 06/13/16 Pct Recovery = 92% Analysis Date = 06/13/16 Pct Recovery = 92% Analysis Date = 06/08/16 Pct Recovery = 93% Analysis Date = 06/08/16 Pct Recovery = 93% Analysis Date = 06/04/16 Pct Recovery = 93% Analysis Date = 06/04/16 Pct Recovery = 93% Analysis Date = 05/30/16 Pct Recovery = 93% Analysis Date = 05/30/16 Pct Recovery = 93% Analysis Date = 05/25/16 Pct Recovery = 93% Analysis Date = 05/25/16 Pct Recovery = 93% Analysis Date = 05/20/16 Pct Recovery = 94% Analysis Date = 05/20/16 Pct Recovery = 94% Analysis Date = 05/16/16 Pct Recovery = 94% Analysis Date = 05/16/16 Pct Recovery = 94% Analysis Date = 05/11/16 Pct Recovery = 94% Analysis Date = 05/11/16 Pct Recovery = 94% Analysis Date = 05/06/16 Pct Recovery = 94% Analysis Date = 05/06/16 Pct Recovery = 94% Analysis Date = 05/01/16 Pct Recovery = 95% Analysis Date = 05/01/16 Pct Recovery = 95% Analysis Date = 04/27/16 Pct Recovery = 95% Analysis Date = 04/27/16 Pct Recovery = 95% Analysis Date = 04/22/16 Pct Recovery = 95% Analysis Date = 04/22/16 Pct Recovery = 95% Analysis Date = 04/17/16 Pct Recovery = 95% Analysis Date = 04/17/16 Pct Recovery = 95% Analysis Date = 04/12/16 Pct Recovery = 95% Analysis Date = 04/12/16 Pct Recovery = 95% Analysis Date = 04/07/16 Pct Recovery = 96% Analysis Date = 04/07/16 Pct Recovery = 96% Analysis Date = 04/03/16 Pct Recovery = 96% Analysis Date = 04/03/16 Pct Recovery = 96% Analysis Date = 03/29/16 Pct Recovery = 96% Analysis Date = 03/29/16 Pct Recovery = 96% Analysis Date = 03/24/16 Pct Recovery = 96% Analysis Date = 03/24/16 Pct Recovery = 96% Analysis Date = 03/19/16 Pct Recovery = 96% Analysis Date = 03/19/16 Pct Recovery = 96% Analysis Date = 03/15/16 Pct Recovery = 96% Analysis Date = 03/15/16 Pct Recovery = 96% Analysis Date = 03/10/16 Pct Recovery = 97% Analysis Date = 03/10/16 Pct Recovery = 97% Analysis Date = 03/05/16 Pct Recovery = 97% Analysis Date = 03/05/16 Pct Recovery = 97% Analysis Date = 02/29/16 Pct Recovery = 97% Analysis Date = 02/29/16 Pct Recovery = 97% Analysis Date = 02/25/16 Pct Recovery = 97% Analysis Date = 02/25/16 Pct Recovery = 97% Analysis Date = 02/20/16 Pct Recovery = 97% Analysis Date = 02/20/16 Pct Recovery = 97% Analysis Date = 02/15/16 Pct Recovery = 98% Analysis Date = 02/15/16 Pct Recovery = 98% Analysis Date = 02/10/16 Pct Recovery = 98% Analysis Date = 02/10/16 Pct Recovery = 98% Analysis Date = 02/05/16 Pct Recovery = 98% Analysis Date = 02/05/16 Pct Recovery = 98% Analysis Date = 02/01/16 Pct Recovery = 98% Analysis Date = 02/01/16 Pct Recovery = 98% Analysis Date = 01/27/16 Pct Recovery = 98% Analysis Date = 01/27/16 Pct Recovery = 98% Analysis Date = 01/22/16 Pct Recovery = 98% Analysis Date = 01/22/16 Pct Recovery = 98% Analysis Date = 01/17/16 Pct Recovery = 98% Analysis Date = 01/17/16 Pct Recovery = 98% Analysis Date = 01/13/16 Pct Recovery = 98% Analysis Date = 01/13/16 Pct Recovery = 98% Analysis Date = 01/08/16 Pct Recovery = 98% Analysis Date = 01/08/16 Pct Recovery = 98% Analysis Date = 01/03/16 Pct Recovery = 98% Analysis Date = 01/03/16 Pct Recovery = 98% Analysis Date = 12/29/15 Pct Recovery = 98% Analysis Date = 12/29/15 Pct Recovery = 98% Analysis Date = 12/25/15 Pct Recovery = 98% Analysis Date = 12/25/15 Pct Recovery = 98% Analysis Date = 12/20/15 Pct Recovery = 98% Analysis Date = 12/20/15 Pct Recovery = 98% Analysis Date = 12/15/15 Pct Recovery = 99% Analysis Date = 12/15/15 Pct Recovery = 99% Analysis Date = 12/10/15 Pct Recovery = 99% Analysis Date = 12/10/15 Pct Recovery = 99% Analysis Date = 12/05/15 Pct Recovery = 98% Analysis Date = 12/05/15 Pct Recovery = 98% Analysis Date = 12/01/15 Pct Recovery = 98% Analysis Date = 12/01/15 Pct Recovery = 98% Analysis Date = 11/26/15 Pct Recovery = 98% Analysis Date = 11/26/15 Pct Recovery = 98% Analysis Date = 11/21/15 Pct Recovery = 98% Analysis Date = 11/21/15 Pct Recovery = 98% Analysis Date = 11/16/15 Pct Recovery = 98% Analysis Date = 11/16/15 Pct Recovery = 98% Analysis Date = 11/12/15 Pct Recovery = 98% Analysis Date = 11/12/15 Pct Recovery = 98% Analysis Date = 11/07/15 Pct Recovery = 98% Analysis Date = 11/07/15 Pct Recovery = 98% Analysis Date = 11/02/15 Pct Recovery = 97% Analysis Date = 11/02/15 Pct Recovery = 97% Analysis Date = 10/28/15 Pct Recovery = 97% Analysis Date = 10/28/15 Pct Recovery = 97% Analysis Date = 10/24/15 Pct Recovery = 97% Analysis Date = 10/24/15 Pct Recovery = 97% Analysis Date = 10/19/15 Pct Recovery = 97% Analysis Date = 10/19/15 Pct Recovery = 97% Analysis Date = 10/14/15 Pct Recovery = 97% Analysis Date = 10/14/15 Pct Recovery = 97% Analysis Date = 10/09/15 Pct Recovery = 97% Analysis Date = 10/09/15 Pct Recovery = 97% Analysis Date = 10/04/15 Pct Recovery = 96% Analysis Date = 10/04/15 Pct Recovery = 96% Analysis Date = 09/30/15 Pct Recovery = 96% Analysis Date = 09/30/15 Pct Recovery = 96% Analysis Date = 09/25/15 Pct Recovery = 96% Analysis Date = 09/25/15 Pct Recovery = 96% Analysis Date = 09/20/15 Pct Recovery = 96% Analysis Date = 09/20/15 Pct Recovery = 96% Analysis Date = 09/15/15 Pct Recovery = 96% Analysis Date = 09/15/15 Pct Recovery = 96% Analysis Date = 09/11/15 Pct Recovery = 96% Analysis Date = 09/11/15 Pct Recovery = 96% Analysis Date = 09/06/15 Pct Recovery = 95% Analysis Date = 09/06/15 Pct Recovery = 95% Analysis Date = 09/01/15 Pct Recovery = 95% Analysis Date = 09/01/15 Pct Recovery = 95% Analysis Date = 08/27/15 Pct Recovery = 95% Analysis Date = 08/27/15 Pct Recovery = 95% Analysis Date = 08/23/15 Pct Recovery = 95% Analysis Date = 08/23/15 Pct Recovery = 95% Analysis Date = 08/18/15 Pct Recovery = 95% Analysis Date = 08/18/15 Pct Recovery = 95% Analysis Date = 08/13/15 Pct Recovery = 95% Analysis Date = 08/13/15 Pct Recovery = 95% Analysis Date = 08/08/15 Pct Recovery = 94% Analysis Date = 08/08/15 Pct Recovery = 94% Analysis Date = 08/03/15 Pct Recovery = 94% Analysis Date = 08/03/15 Pct Recovery = 94% Analysis Date = 07/30/15 Pct Recovery = 94% Analysis Date = 07/30/15 Pct Recovery = 94% Analysis Date = 07/25/15 Pct Recovery = 94% Analysis Date = 07/25/15 Pct Recovery = 94% Analysis Date = 07/20/15 Pct Recovery = 94% Analysis Date = 07/20/15 Pct Recovery = 94% Analysis Date = 07/15/15 Pct Recovery = 94% Analysis Date = 07/15/15 Pct Recovery = 94% Analysis Date = 07/11/15 Pct Recovery = 93% Analysis Date = 07/11/15 Pct Recovery = 93% Analysis Date = 07/06/15 Pct Recovery = 93% Analysis Date = 07/06/15 Pct Recovery = 93% Analysis Date = 07/01/15 Pct Recovery = 93% Analysis Date = 07/01/15 Pct Recovery = 93% Analysis Date = 06/26/15 Pct Recovery = 93% Analysis Date = 06/26/15 Pct Recovery = 93% Analysis Date = 06/21/15 Pct Recovery = 93% Analysis Date = 06/21/15 Pct Recovery = 93% Analysis Date = 06/17/15 Pct Recovery = 93% Analysis Date = 06/17/15 Pct Recovery = 93% Analysis Date = 06/12/15 Pct Recovery = 93% Analysis Date = 06/12/15 Pct Recovery = 93% Analysis Date = 06/07/15 Pct Recovery = 93% Analysis Date = 06/07/15 Pct Recovery = 93% Analysis Date = 06/02/15 Pct Recovery = 93% Analysis Date = 06/02/15 Pct Recovery = 93% Analysis Date = 05/29/15 Pct Recovery = 93% Analysis Date = 05/29/15 Pct Recovery = 93% Analysis Date = 05/24/15 Pct Recovery = 93% Analysis Date = 05/24/15 Pct Recovery = 93% Analysis Date = 05/19/15 Pct Recovery = 93% Analysis Date = 05/19/15 Pct Recovery = 93% Analysis Date = 05/14/15 Pct Recovery = 93% Analysis Date = 05/14/15 Pct Recovery = 93% Analysis Date = 05/10/15 Pct Recovery = 92% Analysis Date = 05/10/15 Pct Recovery = 92% Analysis Date = 05/05/15 Pct Recovery = 92% Analysis Date = 05/05/15 Pct Recovery = 92% Analysis Date = 04/30/15 Pct Recovery = 92% Analysis Date = 04/30/15 Pct Recovery = 92% Analysis Date = 04/25/15 Pct Recovery = 92% Analysis Date = 04/25/15 Pct Recovery = 92% Analysis Date = 04/20/15 Pct Recovery = 92% Analysis Date = 04/20/15 Pct Recovery = 92% Analysis Date = 04/16/15 Pct Recovery = 92% Analysis Date = 04/16/15 Pct Recovery = 92% Analysis Date = 04/11/15 Pct Recovery = 92% Analysis Date = 04/11/15 Pct Recovery = 92% Analysis Date = 04/06/15 Pct Recovery = 92% Analysis Date = 04/06/15 Pct Recovery = 92% Analysis Date = 04/01/15 Pct Recovery = 92% Analysis Date = 04/01/15 Pct Recovery = 92% Analysis Date = 03/28/15 Pct Recovery = 92% Analysis Date = 03/28/15 Pct Recovery = 92% Analysis Date = 03/23/15 Pct Recovery = 92% Analysis Date = 03/23/15 Pct Recovery = 92% Analysis Date = 03/18/15 Pct Recovery = 92% Analysis Date = 03/18/15 Pct Recovery = 92% Analysis Date = 03/13/15 Pct Recovery = 92% Analysis Date = 03/13/15 Pct Recovery = 92% Analysis Date = 03/09/15 Pct Recovery = 92% Analysis Date = 03/09/15 Pct Recovery = 92% Analysis Date = 03/04/15 Pct Recovery = 92% Analysis Date = 03/04/15 Pct Recovery = 92% Analysis Date = 02/27/15 Pct Recovery = 92% Analysis Date = 02/27/15 Pct Recovery = 92% Analysis Date = 02/22/15 Pct Recovery = 92% Analysis Date = 02/22/15 Pct Recovery = 92% Analysis Date = 02/17/15 Pct Recovery = 92% Analysis Date = 02/17/15 Pct Recovery = 92% Analysis Date = 02/13/15 Pct Recovery = 92% Analysis Date = 02/13/15 Pct Recovery = 92% Analysis Date = 02/08/15 Pct Recovery = 92% Analysis Date = 02/08/15 Pct Recovery = 92% Analysis Date = 02/03/15 Pct Recovery = 92% Analysis Date = 02/03/15 Pct Recovery = 92% Analysis Date = 01/29/15 Pct Recovery = 92% Analysis Date = 01/29/15 Pct Recovery = 92% Analysis Date = 01/25/15 Pct Recovery = 92% Analysis Date = 01/25/15 Pct Recovery = 92% Analysis Date = 01/20/15 Pct Recovery = 92% Analysis Date = 01/20/15 Pct Recovery = 92% Analysis Date = 01/15/15 Pct Recovery = 93% Analysis Date = 01/15/15 Pct Recovery = 93% Analysis Date = 01/10/15 Pct Recovery = 93% Analysis Date = 01/10/15 Pct Recovery = 93% Analysis Date = 01/06/15 Pct Recovery = 93% Analysis Date = 01/06/15 Pct Recovery = 93% Analysis Date = 01/01/15 Pct Recovery = 93% Analysis Date = 01/01/15 Pct Recovery = 93% Analysis Date = 12/27/14 Pct Recovery = 93% Analysis Date = 12/27/14 Pct Recovery = 93% Analysis Date = 12/22/14 Pct Recovery = 93% Analysis Date = 12/22/14 Pct Recovery = 93% Analysis Date = 12/17/14 Pct Recovery = 93% Analysis Date = 12/17/14 Pct Recovery = 93% Analysis Date = 12/13/14 Pct Recovery = 93% Analysis Date = 12/13/14 Pct Recovery = 93% Analysis Date = 12/08/14 Pct Recovery = 93% Analysis Date = 12/08/14 Pct Recovery = 93% Analysis Date = 12/03/14 Pct Recovery = 93% Analysis Date = 12/03/14 Pct Recovery = 93% Analysis Date = 11/28/14 Pct Recovery = 93% Analysis Date = 11/28/14 Pct Recovery = 93% Analysis Date = 11/24/14 Pct Recovery = 93% Analysis Date = 11/24/14 Pct Recovery = 93% Analysis Date = 11/19/14 Pct Recovery = 93% Analysis Date = 11/19/14 Pct Recovery = 93% Analysis Date = 11/14/14 Pct Recovery = 93% Analysis Date = 11/14/14 Pct Recovery = 93% Analysis Date = 11/09/14 Pct Recovery = 93% Analysis Date = 11/09/14 Pct Recovery = 93% Analysis Date = 11/05/14 Pct Recovery = 93% Analysis Date = 11/05/14 Pct Recovery = 93% Analysis Date = 10/31/14 Pct Recovery = 93% Analysis Date = 10/31/14 Pct Recovery = 93% Analysis Date = 10/26/14 Pct Recovery = 93% Analysis Date = 10/26/14 Pct Recovery = 93% Analysis Date = 10/21/14 Pct Recovery = 94% Analysis Date = 10/21/14 Pct Recovery = 94% Analysis Date = 10/16/14 Pct Recovery = 94% Analysis Date = 10/16/14 Pct Recovery = 94% Analysis Date = 10/12/14 Pct Recovery = 94% Analysis Date = 10/12/14 Pct Recovery = 94% Analysis Date = 10/07/14 Pct Recovery = 94% Analysis Date = 10/07/14 Pct Recovery = 94% Analysis Date = 10/02/14 Pct Recovery = 94% Analysis Date = 10/02/14 Pct Recovery = 94% Analysis Date = 09/27/14 Pct Recovery = 94% Analysis Date = 09/27/14 Pct Recovery = 94% Analysis Date = 09/23/14 Pct Recovery = 94% Analysis Date = 09/23/14 Pct Recovery = 94% Analysis Date = 09/18/14 Pct Recovery = 94% Analysis Date = 09/18/14 Pct Recovery = 94% Analysis Date = 09/13/14 Pct Recovery = 94% Analysis Date = 09/13/14 Pct Recovery = 94% Analysis Date = 09/08/14 Pct Recovery = 94% Analysis Date = 09/08/14 Pct Recovery = 94% Analysis Date = 09/04/14 Pct Recovery = 94% Analysis Date = 09/04/14 Pct Recovery = 94% Analysis Date = 08/30/14 Pct Recovery = 94% Analysis Date = 08/30/14 Pct Recovery = 94% Analysis Date = 08/25/14 Pct Recovery = 94% Analysis Date = 08/25/14 Pct Recovery = 94% Analysis Date = 08/20/14 Pct Recovery = 94% Analysis Date = 08/20/14 Pct Recovery = 94% Analysis Date = 08/15/14 Pct Recovery = 95% Analysis Date = 08/15/14 Pct Recovery = 95% Analysis Date = 08/11/14 Pct Recovery = 95% Analysis Date = 08/11/14 Pct Recovery = 95% Analysis Date = 08/06/14 Pct Recovery = 95% Analysis Date = 08/06/14 Pct Recovery = 95% Analysis Date = 08/01/14 Pct Recovery = 95% Analysis Date = 08/01/14 Pct Recovery = 95% Analysis Date = 07/27/14 Pct Recovery = 95% Analysis Date = 07/27/14 Pct Recovery = 95% Analysis Date = 07/23/14 Pct Recovery = 95% Analysis Date = 07/23/14 Pct Recovery = 95% Analysis Date = 07/18/14 Pct Recovery = 95% Analysis Date = 07/18/14 Pct Recovery = 95% Analysis Date = 07/13/14 Pct Recovery = 95% Analysis Date = 07/13/14 Pct Recovery = 95% Analysis Date = 07/08/14 Pct Recovery = 95% Analysis Date = 07/08/14 Pct Recovery = 95% Analysis Date = 07/04/14 Pct Recovery = 95% Analysis Date = 07/04/14 Pct Recovery = 95% Analysis Date = 06/29/14 Pct Recovery = 95% Analysis Date = 06/29/14 Pct Recovery = 95% Analysis Date = 06/24/14 Pct Recovery = 96% Analysis Date = 06/24/14 Pct Recovery = 96% Analysis Date = 06/19/14 Pct Recovery = 96% Analysis Date = 06/19/14 Pct Recovery = 96% Analysis Date = 06/14/14 Pct Recovery = 96% Analysis Date = 06/14/14 Pct Recovery = 96% Analysis Date = 06/10/14 Pct Recovery = 96% Analysis Date = 06/10/14 Pct Recovery = 96% Analysis Date = 06/05/14 Pct Recovery = 96% Analysis Date = 06/05/14 Pct Recovery = 96% Analysis Date = 05/31/14 Pct Recovery = 96% Analysis Date = 05/31/14 Pct Recovery = 96% Analysis Date = 05/26/14 Pct Recovery = 96% Analysis Date = 05/26/14 Pct Recovery = 96% Analysis Date = 05/22/14 Pct Recovery = 96% Analysis Date = 05/22/14 Pct Recovery = 96% Analysis Date = 05/17/14 Pct Recovery = 96% Analysis Date = 05/17/14 Pct Recovery = 96% Analysis Date = 05/12/14 Pct Recovery = 96% Analysis Date = 05/12/14 Pct Recovery = 96% Analysis Date = 05/07/14 Pct Recovery = 97% Analysis Date = 05/07/14 Pct Recovery = 97% Analysis Date = 05/03/14 Pct Recovery = 97% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
HEXACHLOROETHANE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 48 93% 12% 92% 10%
Total 48 93% 12% 92% 10%

Sample Statistics
HEXACHLOROETHANE

Characteristic N % % Basis
Plotted 48 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 48 .  
False Negatives 0 0% 0 out of 48
Not Spiked 25 .  
False Positives 0 0% 0 out of 25

BQS OBSP Determination:
HEXANE
METHOD: 4440 , TESTIDCODE: 81590GCM66
Open Data Set

Analysis Date = 12/12/16 SpikeMix = Accu 216041125: 40 µl & Crescent 03FF058: 40 µl Pct Recovery = 88% Analysis Date = 07/20/16 SpikeMix = Supelco LC20141V: 40 µl & Accu 216041125: 40 µl Pct Recovery = 126% Analysis Date = 07/14/16 SpikeMix = Accu 216041125: 40 µl & NSI 041816AVOC: 40 µl Pct Recovery = 98% Analysis Date = 08/12/16 SpikeMix = ChemService 5082900: 25 µl & Phenova B20160319: 25 µl Pct Recovery = 84% Analysis Date = 06/21/16 SpikeMix = Phenova B20160319: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 84% Analysis Date = 09/08/16 SpikeMix = Supelco LC20141V: 25 µl & Accu 216041125: 25 µl Pct Recovery = 89% Analysis Date = 05/24/16 SpikeMix = Accu 216041125: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 71% Analysis Date = 03/19/15 SpikeMix = Spex Organics C1140417015: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 141% Analysis Date = 11/22/14 SpikeMix = NSI 032614: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 148% Analysis Date = 08/19/14 SpikeMix = Spex Organics C1140417015: 20 µl & Accu 214031115: 20 µl Pct Recovery = 167% Analysis Date = 08/16/14 SpikeMix = ERA 0227-14-06.1A: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 136% Analysis Date = 08/15/15 SpikeMix = Supelco LC13545: 25 µl & Crescent 04EE008: 25 µl Pct Recovery = 92% Analysis Date = 06/16/15 SpikeMix = ERA 0406-15-03: 25 µl & Supelco LC13545: 25 µl Pct Recovery = 79% Analysis Date = 11/29/16 SpikeMix = ChemService 5082900: 15 µl & Phenova B20160319: 15 µl Pct Recovery = 66% Analysis Date = 09/08/16 SpikeMix = Phenova B20160319: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 93% Analysis Date = 07/29/16 SpikeMix = Phenova B20160319: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 113% Analysis Date = 05/27/16 SpikeMix = Phenova B20160319: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 86% Analysis Date = 10/13/16 SpikeMix = Accu 216041125: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 118% Analysis Date = 08/20/16 SpikeMix = Accu 216041125: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 107% Analysis Date = 06/30/16 SpikeMix = ChemService 5082900: 15 µl & Accu 216041125: 15 µl Pct Recovery = 64% Analysis Date = 04/26/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 78% Analysis Date = 04/02/16 SpikeMix = Supelco LC13545: 15 µl & Accu 215041380: 15 µl Pct Recovery = 87% Analysis Date = 02/05/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 94% Analysis Date = 12/18/15 SpikeMix = Supelco LC13545: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 95% Analysis Date = 11/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 98% Analysis Date = 10/16/15 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 97% Analysis Date = 05/09/15 SpikeMix = Spex Organics EN150428007: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 113% Analysis Date = 11/06/14 SpikeMix = Spex Organics C1140417015: 10 µl & Crescent 03DD004: 10 µl Pct Recovery = 133% Analysis Date = 09/09/14 SpikeMix = NSI 032614: 10 µl & Spex Organics C1140417015: 10 µl Pct Recovery = 170% Analysis Date = 07/23/14 SpikeMix = Spex Organics C1140417015: 10 µl & Accu 214031115: 10 µl Pct Recovery = 170% Analysis Date = 07/11/14 SpikeMix = Spex Organics C1140417015: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 148% Analysis Date = 05/13/16 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 76% Analysis Date = 03/17/16 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 83% Analysis Date = 02/18/16 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 121% Analysis Date = 12/10/15 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 104% Analysis Date = 11/12/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 91% Analysis Date = 09/03/15 SpikeMix = NSI 050515AVOC: 10 µl & Spex Organics EN150428007: 10 µl Pct Recovery = 86% Analysis Date = 06/27/15 SpikeMix = ERA 0406-15-03: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 79% Analysis Date = 05/21/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 101% Analysis Date = 05/09/15 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 90% Analysis Date = 12/11/16 Pct Recovery = 93% Analysis Date = 12/07/16 Pct Recovery = 93% Analysis Date = 12/07/16 Pct Recovery = 93% Analysis Date = 12/03/16 Pct Recovery = 93% Analysis Date = 12/03/16 Pct Recovery = 93% Analysis Date = 11/28/16 Pct Recovery = 93% Analysis Date = 11/28/16 Pct Recovery = 93% Analysis Date = 11/24/16 Pct Recovery = 93% Analysis Date = 11/24/16 Pct Recovery = 93% Analysis Date = 11/19/16 Pct Recovery = 93% Analysis Date = 11/19/16 Pct Recovery = 93% Analysis Date = 11/15/16 Pct Recovery = 93% Analysis Date = 11/15/16 Pct Recovery = 93% Analysis Date = 11/11/16 Pct Recovery = 93% Analysis Date = 11/11/16 Pct Recovery = 93% Analysis Date = 11/06/16 Pct Recovery = 93% Analysis Date = 11/06/16 Pct Recovery = 93% Analysis Date = 11/02/16 Pct Recovery = 93% Analysis Date = 11/02/16 Pct Recovery = 93% Analysis Date = 10/28/16 Pct Recovery = 93% Analysis Date = 10/28/16 Pct Recovery = 93% Analysis Date = 10/24/16 Pct Recovery = 93% Analysis Date = 10/24/16 Pct Recovery = 93% Analysis Date = 10/19/16 Pct Recovery = 93% Analysis Date = 10/19/16 Pct Recovery = 93% Analysis Date = 10/15/16 Pct Recovery = 93% Analysis Date = 10/15/16 Pct Recovery = 93% Analysis Date = 10/11/16 Pct Recovery = 92% Analysis Date = 10/11/16 Pct Recovery = 92% Analysis Date = 10/06/16 Pct Recovery = 92% Analysis Date = 10/06/16 Pct Recovery = 92% Analysis Date = 10/02/16 Pct Recovery = 92% Analysis Date = 10/02/16 Pct Recovery = 92% Analysis Date = 09/27/16 Pct Recovery = 92% Analysis Date = 09/27/16 Pct Recovery = 92% Analysis Date = 09/23/16 Pct Recovery = 92% Analysis Date = 09/23/16 Pct Recovery = 92% Analysis Date = 09/18/16 Pct Recovery = 92% Analysis Date = 09/18/16 Pct Recovery = 92% Analysis Date = 09/14/16 Pct Recovery = 92% Analysis Date = 09/14/16 Pct Recovery = 92% Analysis Date = 09/10/16 Pct Recovery = 92% Analysis Date = 09/10/16 Pct Recovery = 92% Analysis Date = 09/05/16 Pct Recovery = 92% Analysis Date = 09/05/16 Pct Recovery = 92% Analysis Date = 09/01/16 Pct Recovery = 92% Analysis Date = 09/01/16 Pct Recovery = 92% Analysis Date = 08/27/16 Pct Recovery = 92% Analysis Date = 08/27/16 Pct Recovery = 92% Analysis Date = 08/23/16 Pct Recovery = 92% Analysis Date = 08/23/16 Pct Recovery = 92% Analysis Date = 08/18/16 Pct Recovery = 92% Analysis Date = 08/18/16 Pct Recovery = 92% Analysis Date = 08/14/16 Pct Recovery = 92% Analysis Date = 08/14/16 Pct Recovery = 92% Analysis Date = 08/10/16 Pct Recovery = 92% Analysis Date = 08/10/16 Pct Recovery = 92% Analysis Date = 08/05/16 Pct Recovery = 92% Analysis Date = 08/05/16 Pct Recovery = 92% Analysis Date = 08/01/16 Pct Recovery = 92% Analysis Date = 08/01/16 Pct Recovery = 92% Analysis Date = 07/27/16 Pct Recovery = 92% Analysis Date = 07/27/16 Pct Recovery = 92% Analysis Date = 07/23/16 Pct Recovery = 92% Analysis Date = 07/23/16 Pct Recovery = 92% Analysis Date = 07/18/16 Pct Recovery = 92% Analysis Date = 07/18/16 Pct Recovery = 92% Analysis Date = 07/14/16 Pct Recovery = 92% Analysis Date = 07/14/16 Pct Recovery = 92% Analysis Date = 07/10/16 Pct Recovery = 92% Analysis Date = 07/10/16 Pct Recovery = 92% Analysis Date = 07/05/16 Pct Recovery = 92% Analysis Date = 07/05/16 Pct Recovery = 92% Analysis Date = 07/01/16 Pct Recovery = 91% Analysis Date = 07/01/16 Pct Recovery = 91% Analysis Date = 06/26/16 Pct Recovery = 91% Analysis Date = 06/26/16 Pct Recovery = 91% Analysis Date = 06/22/16 Pct Recovery = 91% Analysis Date = 06/22/16 Pct Recovery = 91% Analysis Date = 06/17/16 Pct Recovery = 91% Analysis Date = 06/17/16 Pct Recovery = 91% Analysis Date = 06/13/16 Pct Recovery = 91% Analysis Date = 06/13/16 Pct Recovery = 91% Analysis Date = 06/09/16 Pct Recovery = 91% Analysis Date = 06/09/16 Pct Recovery = 91% Analysis Date = 06/04/16 Pct Recovery = 91% Analysis Date = 06/04/16 Pct Recovery = 91% Analysis Date = 05/31/16 Pct Recovery = 91% Analysis Date = 05/31/16 Pct Recovery = 91% Analysis Date = 05/26/16 Pct Recovery = 91% Analysis Date = 05/26/16 Pct Recovery = 91% Analysis Date = 05/22/16 Pct Recovery = 91% Analysis Date = 05/22/16 Pct Recovery = 91% Analysis Date = 05/18/16 Pct Recovery = 91% Analysis Date = 05/18/16 Pct Recovery = 91% Analysis Date = 05/13/16 Pct Recovery = 91% Analysis Date = 05/13/16 Pct Recovery = 91% Analysis Date = 05/09/16 Pct Recovery = 91% Analysis Date = 05/09/16 Pct Recovery = 91% Analysis Date = 05/04/16 Pct Recovery = 91% Analysis Date = 05/04/16 Pct Recovery = 91% Analysis Date = 04/30/16 Pct Recovery = 91% Analysis Date = 04/30/16 Pct Recovery = 91% Analysis Date = 04/25/16 Pct Recovery = 91% Analysis Date = 04/25/16 Pct Recovery = 91% Analysis Date = 04/21/16 Pct Recovery = 91% Analysis Date = 04/21/16 Pct Recovery = 91% Analysis Date = 04/17/16 Pct Recovery = 91% Analysis Date = 04/17/16 Pct Recovery = 91% Analysis Date = 04/12/16 Pct Recovery = 91% Analysis Date = 04/12/16 Pct Recovery = 91% Analysis Date = 04/08/16 Pct Recovery = 91% Analysis Date = 04/08/16 Pct Recovery = 91% Analysis Date = 04/03/16 Pct Recovery = 91% Analysis Date = 04/03/16 Pct Recovery = 91% Analysis Date = 03/30/16 Pct Recovery = 91% Analysis Date = 03/30/16 Pct Recovery = 91% Analysis Date = 03/25/16 Pct Recovery = 92% Analysis Date = 03/25/16 Pct Recovery = 92% Analysis Date = 03/21/16 Pct Recovery = 92% Analysis Date = 03/21/16 Pct Recovery = 92% Analysis Date = 03/17/16 Pct Recovery = 92% Analysis Date = 03/17/16 Pct Recovery = 92% Analysis Date = 03/12/16 Pct Recovery = 92% Analysis Date = 03/12/16 Pct Recovery = 92% Analysis Date = 03/08/16 Pct Recovery = 92% Analysis Date = 03/08/16 Pct Recovery = 92% Analysis Date = 03/03/16 Pct Recovery = 92% Analysis Date = 03/03/16 Pct Recovery = 92% Analysis Date = 02/28/16 Pct Recovery = 92% Analysis Date = 02/28/16 Pct Recovery = 92% Analysis Date = 02/23/16 Pct Recovery = 92% Analysis Date = 02/23/16 Pct Recovery = 92% Analysis Date = 02/19/16 Pct Recovery = 92% Analysis Date = 02/19/16 Pct Recovery = 92% Analysis Date = 02/15/16 Pct Recovery = 92% Analysis Date = 02/15/16 Pct Recovery = 92% Analysis Date = 02/10/16 Pct Recovery = 92% Analysis Date = 02/10/16 Pct Recovery = 92% Analysis Date = 02/06/16 Pct Recovery = 92% Analysis Date = 02/06/16 Pct Recovery = 92% Analysis Date = 02/01/16 Pct Recovery = 93% Analysis Date = 02/01/16 Pct Recovery = 93% Analysis Date = 01/28/16 Pct Recovery = 93% Analysis Date = 01/28/16 Pct Recovery = 93% Analysis Date = 01/23/16 Pct Recovery = 93% Analysis Date = 01/23/16 Pct Recovery = 93% Analysis Date = 01/19/16 Pct Recovery = 93% Analysis Date = 01/19/16 Pct Recovery = 93% Analysis Date = 01/15/16 Pct Recovery = 93% Analysis Date = 01/15/16 Pct Recovery = 93% Analysis Date = 01/10/16 Pct Recovery = 93% Analysis Date = 01/10/16 Pct Recovery = 93% Analysis Date = 01/06/16 Pct Recovery = 93% Analysis Date = 01/06/16 Pct Recovery = 93% Analysis Date = 01/01/16 Pct Recovery = 93% Analysis Date = 01/01/16 Pct Recovery = 93% Analysis Date = 12/28/15 Pct Recovery = 93% Analysis Date = 12/28/15 Pct Recovery = 93% Analysis Date = 12/23/15 Pct Recovery = 93% Analysis Date = 12/23/15 Pct Recovery = 93% Analysis Date = 12/19/15 Pct Recovery = 94% Analysis Date = 12/19/15 Pct Recovery = 94% Analysis Date = 12/15/15 Pct Recovery = 94% Analysis Date = 12/15/15 Pct Recovery = 94% Analysis Date = 12/10/15 Pct Recovery = 94% Analysis Date = 12/10/15 Pct Recovery = 94% Analysis Date = 12/06/15 Pct Recovery = 94% Analysis Date = 12/06/15 Pct Recovery = 94% Analysis Date = 12/01/15 Pct Recovery = 94% Analysis Date = 12/01/15 Pct Recovery = 94% Analysis Date = 11/27/15 Pct Recovery = 94% Analysis Date = 11/27/15 Pct Recovery = 94% Analysis Date = 11/23/15 Pct Recovery = 94% Analysis Date = 11/23/15 Pct Recovery = 94% Analysis Date = 11/18/15 Pct Recovery = 94% Analysis Date = 11/18/15 Pct Recovery = 94% Analysis Date = 11/14/15 Pct Recovery = 93% Analysis Date = 11/14/15 Pct Recovery = 93% Analysis Date = 11/09/15 Pct Recovery = 94% Analysis Date = 11/09/15 Pct Recovery = 94% Analysis Date = 11/05/15 Pct Recovery = 94% Analysis Date = 11/05/15 Pct Recovery = 94% Analysis Date = 10/31/15 Pct Recovery = 94% Analysis Date = 10/31/15 Pct Recovery = 94% Analysis Date = 10/27/15 Pct Recovery = 94% Analysis Date = 10/27/15 Pct Recovery = 94% Analysis Date = 10/23/15 Pct Recovery = 94% Analysis Date = 10/23/15 Pct Recovery = 94% Analysis Date = 10/18/15 Pct Recovery = 94% Analysis Date = 10/18/15 Pct Recovery = 94% Analysis Date = 10/14/15 Pct Recovery = 95% Analysis Date = 10/14/15 Pct Recovery = 95% Analysis Date = 10/09/15 Pct Recovery = 95% Analysis Date = 10/09/15 Pct Recovery = 95% Analysis Date = 10/05/15 Pct Recovery = 95% Analysis Date = 10/05/15 Pct Recovery = 95% Analysis Date = 09/30/15 Pct Recovery = 95% Analysis Date = 09/30/15 Pct Recovery = 95% Analysis Date = 09/26/15 Pct Recovery = 95% Analysis Date = 09/26/15 Pct Recovery = 95% Analysis Date = 09/22/15 Pct Recovery = 95% Analysis Date = 09/22/15 Pct Recovery = 95% Analysis Date = 09/17/15 Pct Recovery = 96% Analysis Date = 09/17/15 Pct Recovery = 96% Analysis Date = 09/13/15 Pct Recovery = 96% Analysis Date = 09/13/15 Pct Recovery = 96% Analysis Date = 09/08/15 Pct Recovery = 96% Analysis Date = 09/08/15 Pct Recovery = 96% Analysis Date = 09/04/15 Pct Recovery = 96% Analysis Date = 09/04/15 Pct Recovery = 96% Analysis Date = 08/30/15 Pct Recovery = 96% Analysis Date = 08/30/15 Pct Recovery = 96% Analysis Date = 08/26/15 Pct Recovery = 97% Analysis Date = 08/26/15 Pct Recovery = 97% Analysis Date = 08/22/15 Pct Recovery = 97% Analysis Date = 08/22/15 Pct Recovery = 97% Analysis Date = 08/17/15 Pct Recovery = 98% Analysis Date = 08/17/15 Pct Recovery = 98% Analysis Date = 08/13/15 Pct Recovery = 98% Analysis Date = 08/13/15 Pct Recovery = 98% Analysis Date = 08/08/15 Pct Recovery = 98% Analysis Date = 08/08/15 Pct Recovery = 98% Analysis Date = 08/04/15 Pct Recovery = 99% Analysis Date = 08/04/15 Pct Recovery = 99% Analysis Date = 07/30/15 Pct Recovery = 99% Analysis Date = 07/30/15 Pct Recovery = 99% Analysis Date = 07/26/15 Pct Recovery = 99% Analysis Date = 07/26/15 Pct Recovery = 99% Analysis Date = 07/22/15 Pct Recovery = 100% Analysis Date = 07/22/15 Pct Recovery = 100% Analysis Date = 07/17/15 Pct Recovery = 100% Analysis Date = 07/17/15 Pct Recovery = 100% Analysis Date = 07/13/15 Pct Recovery = 101% Analysis Date = 07/13/15 Pct Recovery = 101% Analysis Date = 07/08/15 Pct Recovery = 101% Analysis Date = 07/08/15 Pct Recovery = 101% Analysis Date = 07/04/15 Pct Recovery = 101% Analysis Date = 07/04/15 Pct Recovery = 101% Analysis Date = 06/29/15 Pct Recovery = 102% Analysis Date = 06/29/15 Pct Recovery = 102% Analysis Date = 06/25/15 Pct Recovery = 102% Analysis Date = 06/25/15 Pct Recovery = 102% Analysis Date = 06/21/15 Pct Recovery = 103% Analysis Date = 06/21/15 Pct Recovery = 103% Analysis Date = 06/16/15 Pct Recovery = 104% Analysis Date = 06/16/15 Pct Recovery = 104% Analysis Date = 06/12/15 Pct Recovery = 104% Analysis Date = 06/12/15 Pct Recovery = 104% Analysis Date = 06/07/15 Pct Recovery = 105% Analysis Date = 06/07/15 Pct Recovery = 105% Analysis Date = 06/03/15 Pct Recovery = 106% Analysis Date = 06/03/15 Pct Recovery = 106% Analysis Date = 05/30/15 Pct Recovery = 106% Analysis Date = 05/30/15 Pct Recovery = 106% Analysis Date = 05/25/15 Pct Recovery = 107% Analysis Date = 05/25/15 Pct Recovery = 107% Analysis Date = 05/21/15 Pct Recovery = 108% Analysis Date = 05/21/15 Pct Recovery = 108% Analysis Date = 05/16/15 Pct Recovery = 108% Analysis Date = 05/16/15 Pct Recovery = 108% Analysis Date = 05/12/15 Pct Recovery = 109% Analysis Date = 05/12/15 Pct Recovery = 109% Analysis Date = 05/07/15 Pct Recovery = 110% Analysis Date = 05/07/15 Pct Recovery = 110% Analysis Date = 05/03/15 Pct Recovery = 110% Analysis Date = 05/03/15 Pct Recovery = 110% Analysis Date = 04/29/15 Pct Recovery = 111% Analysis Date = 04/29/15 Pct Recovery = 111% Analysis Date = 04/24/15 Pct Recovery = 112% Analysis Date = 04/24/15 Pct Recovery = 112% Analysis Date = 04/20/15 Pct Recovery = 113% Analysis Date = 04/20/15 Pct Recovery = 113% Analysis Date = 04/15/15 Pct Recovery = 114% Analysis Date = 04/15/15 Pct Recovery = 114% Analysis Date = 04/11/15 Pct Recovery = 114% Analysis Date = 04/11/15 Pct Recovery = 114% Analysis Date = 04/06/15 Pct Recovery = 115% Analysis Date = 04/06/15 Pct Recovery = 115% Analysis Date = 04/02/15 Pct Recovery = 116% Analysis Date = 04/02/15 Pct Recovery = 116% Analysis Date = 03/29/15 Pct Recovery = 117% Analysis Date = 03/29/15 Pct Recovery = 117% Analysis Date = 03/24/15 Pct Recovery = 118% Analysis Date = 03/24/15 Pct Recovery = 118% Analysis Date = 03/20/15 Pct Recovery = 118% Analysis Date = 03/20/15 Pct Recovery = 118% Analysis Date = 03/15/15 Pct Recovery = 119% Analysis Date = 03/15/15 Pct Recovery = 119% Analysis Date = 03/11/15 Pct Recovery = 120% Analysis Date = 03/11/15 Pct Recovery = 120% Analysis Date = 03/06/15 Pct Recovery = 121% Analysis Date = 03/06/15 Pct Recovery = 121% Analysis Date = 03/02/15 Pct Recovery = 121% Analysis Date = 03/02/15 Pct Recovery = 121% Analysis Date = 02/26/15 Pct Recovery = 122% Analysis Date = 02/26/15 Pct Recovery = 122% Analysis Date = 02/21/15 Pct Recovery = 123% Analysis Date = 02/21/15 Pct Recovery = 123% Analysis Date = 02/17/15 Pct Recovery = 124% Analysis Date = 02/17/15 Pct Recovery = 124% Analysis Date = 02/12/15 Pct Recovery = 124% Analysis Date = 02/12/15 Pct Recovery = 124% Analysis Date = 02/08/15 Pct Recovery = 125% Analysis Date = 02/08/15 Pct Recovery = 125% Analysis Date = 02/03/15 Pct Recovery = 126% Analysis Date = 02/03/15 Pct Recovery = 126% Analysis Date = 01/30/15 Pct Recovery = 127% Analysis Date = 01/30/15 Pct Recovery = 127% Analysis Date = 01/26/15 Pct Recovery = 127% Analysis Date = 01/26/15 Pct Recovery = 127% Analysis Date = 01/21/15 Pct Recovery = 128% Analysis Date = 01/21/15 Pct Recovery = 128% Analysis Date = 01/17/15 Pct Recovery = 129% Analysis Date = 01/17/15 Pct Recovery = 129% Analysis Date = 01/12/15 Pct Recovery = 130% Analysis Date = 01/12/15 Pct Recovery = 130% Analysis Date = 01/08/15 Pct Recovery = 131% Analysis Date = 01/08/15 Pct Recovery = 131% Analysis Date = 01/03/15 Pct Recovery = 131% Analysis Date = 01/03/15 Pct Recovery = 131% Analysis Date = 12/30/14 Pct Recovery = 132% Analysis Date = 12/30/14 Pct Recovery = 132% Analysis Date = 12/26/14 Pct Recovery = 133% Analysis Date = 12/26/14 Pct Recovery = 133% Analysis Date = 12/21/14 Pct Recovery = 134% Analysis Date = 12/21/14 Pct Recovery = 134% Analysis Date = 12/17/14 Pct Recovery = 134% Analysis Date = 12/17/14 Pct Recovery = 134% Analysis Date = 12/12/14 Pct Recovery = 135% Analysis Date = 12/12/14 Pct Recovery = 135% Analysis Date = 12/08/14 Pct Recovery = 136% Analysis Date = 12/08/14 Pct Recovery = 136% Analysis Date = 12/04/14 Pct Recovery = 137% Analysis Date = 12/04/14 Pct Recovery = 137% Analysis Date = 11/29/14 Pct Recovery = 137% Analysis Date = 11/29/14 Pct Recovery = 137% Analysis Date = 11/25/14 Pct Recovery = 138% Analysis Date = 11/25/14 Pct Recovery = 138% Analysis Date = 11/20/14 Pct Recovery = 139% Analysis Date = 11/20/14 Pct Recovery = 139% Analysis Date = 11/16/14 Pct Recovery = 140% Analysis Date = 11/16/14 Pct Recovery = 140% Analysis Date = 11/11/14 Pct Recovery = 140% Analysis Date = 11/11/14 Pct Recovery = 140% Analysis Date = 11/07/14 Pct Recovery = 141% Analysis Date = 11/07/14 Pct Recovery = 141% Analysis Date = 11/03/14 Pct Recovery = 142% Analysis Date = 11/03/14 Pct Recovery = 142% Analysis Date = 10/29/14 Pct Recovery = 143% Analysis Date = 10/29/14 Pct Recovery = 143% Analysis Date = 10/25/14 Pct Recovery = 144% Analysis Date = 10/25/14 Pct Recovery = 144% Analysis Date = 10/20/14 Pct Recovery = 144% Analysis Date = 10/20/14 Pct Recovery = 144% Analysis Date = 10/16/14 Pct Recovery = 145% Analysis Date = 10/16/14 Pct Recovery = 145% Analysis Date = 10/11/14 Pct Recovery = 146% Analysis Date = 10/11/14 Pct Recovery = 146% Analysis Date = 10/07/14 Pct Recovery = 147% Analysis Date = 10/07/14 Pct Recovery = 147% Analysis Date = 10/03/14 Pct Recovery = 147% Analysis Date = 10/03/14 Pct Recovery = 147% Analysis Date = 09/28/14 Pct Recovery = 148% Analysis Date = 09/28/14 Pct Recovery = 148% Analysis Date = 09/24/14 Pct Recovery = 149% Analysis Date = 09/24/14 Pct Recovery = 149% Analysis Date = 09/19/14 Pct Recovery = 150% Analysis Date = 09/19/14 Pct Recovery = 150% Analysis Date = 09/15/14 Pct Recovery = 150% Analysis Date = 09/15/14 Pct Recovery = 150% Analysis Date = 09/10/14 Pct Recovery = 151% Analysis Date = 09/10/14 Pct Recovery = 151% Analysis Date = 09/06/14 Pct Recovery = 152% Analysis Date = 09/06/14 Pct Recovery = 152% Analysis Date = 09/02/14 Pct Recovery = 153% Analysis Date = 09/02/14 Pct Recovery = 153% Analysis Date = 08/28/14 Pct Recovery = 154% Analysis Date = 08/28/14 Pct Recovery = 154% Analysis Date = 08/24/14 Pct Recovery = 154% Analysis Date = 08/24/14 Pct Recovery = 154% Analysis Date = 08/19/14 Pct Recovery = 155% Analysis Date = 08/19/14 Pct Recovery = 155% Analysis Date = 08/15/14 Pct Recovery = 156% Analysis Date = 08/15/14 Pct Recovery = 156% Analysis Date = 08/10/14 Pct Recovery = 157% Analysis Date = 08/10/14 Pct Recovery = 157% Analysis Date = 08/06/14 Pct Recovery = 158% Analysis Date = 08/06/14 Pct Recovery = 158% Analysis Date = 08/02/14 Pct Recovery = 158% Analysis Date = 08/02/14 Pct Recovery = 158% Analysis Date = 07/28/14 Pct Recovery = 159% Analysis Date = 07/28/14 Pct Recovery = 159% Analysis Date = 07/24/14 Pct Recovery = 160% Analysis Date = 07/24/14 Pct Recovery = 160% Analysis Date = 07/19/14 Pct Recovery = 161% Analysis Date = 07/19/14 Pct Recovery = 161% Analysis Date = 07/15/14 Pct Recovery = 162% Analysis Date = 07/15/14 Pct Recovery = 162% Analysis Date = 07/11/14 Pct Recovery = 162% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
HEXANE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 40 104% 28% 94% 25%
Total 40 104% 28% 94% 25%

Sample Statistics
HEXANE

Characteristic N % % Basis
Plotted 40 100% Spiked
Estimated Values 40 100% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 40 .  
False Negatives 0 0% 0 out of 40
Not Spiked 25 .  
False Positives 8 32% 8 out of 25

BQS OBSP Determination:
ISOPROPYLBENZENE (CUMENE)
METHOD: 4440 , TESTIDCODE: 77223GCM66
Open Data Set

Analysis Date = 12/16/16 SpikeMix = NSI 041816AVOC: 40 µl & ChemService 5082900: 40 µl Pct Recovery = 84% Analysis Date = 12/12/16 SpikeMix = Accu 216041125: 40 µl & Crescent 03FF058: 40 µl Pct Recovery = 91% Analysis Date = 08/04/16 SpikeMix = Crescent 03FF058: 40 µl & Supelco LC20141V: 40 µl Pct Recovery = 79% Analysis Date = 07/14/16 SpikeMix = Accu 216041125: 40 µl & NSI 041816AVOC: 40 µl Pct Recovery = 85% Analysis Date = 11/21/16 SpikeMix = Crescent 03FF058: 25 µl & Supelco LC20141V: 25 µl Pct Recovery = 86% Analysis Date = 08/26/16 SpikeMix = NSI 041816AVOC: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 79% Analysis Date = 06/30/16 SpikeMix = Crescent 03FF058: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 82% Analysis Date = 06/21/16 SpikeMix = Phenova B20160319: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 86% Analysis Date = 05/24/16 SpikeMix = Accu 216041125: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 79% Analysis Date = 03/19/15 SpikeMix = Spex Organics C1140417015: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 88% Analysis Date = 12/17/14 SpikeMix = Supelco LC06438: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 98% Analysis Date = 11/14/14 SpikeMix = Crescent 03DD004: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 85% Analysis Date = 06/10/14 SpikeMix = Crescent 03DD004: 20 µl & NSI 032614: 20 µl Pct Recovery = 80% Analysis Date = 09/29/15 SpikeMix = Accu 215041380: 25 µl & ERA 0406-15-03: 25 µl Pct Recovery = 82% Analysis Date = 08/15/15 SpikeMix = Supelco LC13545: 25 µl & Crescent 04EE008: 25 µl Pct Recovery = 83% Analysis Date = 07/13/15 SpikeMix = Crescent 04EE008: 25 µl & NSI 050515AVOC: 25 µl Pct Recovery = 80% Analysis Date = 04/09/15 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 89% Analysis Date = 08/19/14 SpikeMix = Spex Organics C1140417015: 20 µl & Accu 214031115: 20 µl Pct Recovery = 103% Analysis Date = 07/01/14 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 99% Analysis Date = 05/01/14 SpikeMix = Accu 214031115: 20 µl & NSI 032614: 20 µl Pct Recovery = 89% Analysis Date = 10/13/16 SpikeMix = Accu 216041125: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 90% Analysis Date = 10/13/16 SpikeMix = NSI 041816AVOC: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 89% Analysis Date = 09/28/16 SpikeMix = Crescent 03FF058: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 84% Analysis Date = 09/08/16 SpikeMix = Phenova B20160319: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 74% Analysis Date = 08/20/16 SpikeMix = Accu 216041125: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 87% Analysis Date = 07/29/16 SpikeMix = Phenova B20160319: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 81% Analysis Date = 06/10/16 SpikeMix = NSI 041816AVOC: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 87% Analysis Date = 04/02/16 SpikeMix = Supelco LC13545: 15 µl & Accu 215041380: 15 µl Pct Recovery = 83% Analysis Date = 03/04/16 SpikeMix = Accu 215041380: 15 µl & ERA 0406-15-03: 15 µl Pct Recovery = 79% Analysis Date = 06/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Accu 215041380: 15 µl Pct Recovery = 86% Analysis Date = 12/18/15 SpikeMix = Supelco LC13545: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 84% Analysis Date = 10/17/15 SpikeMix = Crescent 04EE008: 15 µl & NSI 050515AVOC: 15 µl Pct Recovery = 85% Analysis Date = 05/09/15 SpikeMix = Spex Organics EN150428007: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 90% Analysis Date = 11/06/14 SpikeMix = Spex Organics C1140417015: 10 µl & Crescent 03DD004: 10 µl Pct Recovery = 96% Analysis Date = 10/04/14 SpikeMix = Crescent 03DD004: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 90% Analysis Date = 07/29/14 SpikeMix = Crescent 03DD004: 10 µl & NSI 032614: 10 µl Pct Recovery = 96% Analysis Date = 05/03/14 SpikeMix = Crescent 03DD004: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 117% Analysis Date = 01/13/15 SpikeMix = Accu 214031115: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 107% Analysis Date = 09/09/14 SpikeMix = Accu 214031115: 10 µl & NSI 032614: 10 µl Pct Recovery = 126% Analysis Date = 07/23/14 SpikeMix = Spex Organics C1140417015: 10 µl & Accu 214031115: 10 µl Pct Recovery = 120% Analysis Date = 06/18/14 SpikeMix = Supelco LC06438: 10 µl & Accu 214031115: 10 µl Pct Recovery = 91% Analysis Date = 02/18/16 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 84% Analysis Date = 11/20/15 SpikeMix = Accu 215041380: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 91% Analysis Date = 11/12/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 94% Analysis Date = 05/21/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 100% Analysis Date = 05/13/16 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 89% Analysis Date = 01/27/16 SpikeMix = Crescent 04EE008: 10 µl & NSI 050515AVOC: 10 µl Pct Recovery = 96% Analysis Date = 08/07/15 SpikeMix = Crescent 04EE008: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 92% Analysis Date = 05/09/15 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 93% Analysis Date = 12/15/16 Pct Recovery = 85% Analysis Date = 12/11/16 Pct Recovery = 84% Analysis Date = 12/11/16 Pct Recovery = 84% Analysis Date = 12/06/16 Pct Recovery = 84% Analysis Date = 12/06/16 Pct Recovery = 84% Analysis Date = 12/01/16 Pct Recovery = 84% Analysis Date = 12/01/16 Pct Recovery = 84% Analysis Date = 11/26/16 Pct Recovery = 84% Analysis Date = 11/26/16 Pct Recovery = 84% Analysis Date = 11/21/16 Pct Recovery = 84% Analysis Date = 11/21/16 Pct Recovery = 84% Analysis Date = 11/17/16 Pct Recovery = 84% Analysis Date = 11/17/16 Pct Recovery = 84% Analysis Date = 11/12/16 Pct Recovery = 84% Analysis Date = 11/12/16 Pct Recovery = 84% Analysis Date = 11/07/16 Pct Recovery = 84% Analysis Date = 11/07/16 Pct Recovery = 84% Analysis Date = 11/02/16 Pct Recovery = 84% Analysis Date = 11/02/16 Pct Recovery = 84% Analysis Date = 10/28/16 Pct Recovery = 84% Analysis Date = 10/28/16 Pct Recovery = 84% Analysis Date = 10/24/16 Pct Recovery = 84% Analysis Date = 10/24/16 Pct Recovery = 84% Analysis Date = 10/19/16 Pct Recovery = 84% Analysis Date = 10/19/16 Pct Recovery = 84% Analysis Date = 10/14/16 Pct Recovery = 84% Analysis Date = 10/14/16 Pct Recovery = 84% Analysis Date = 10/09/16 Pct Recovery = 84% Analysis Date = 10/09/16 Pct Recovery = 84% Analysis Date = 10/04/16 Pct Recovery = 84% Analysis Date = 10/04/16 Pct Recovery = 84% Analysis Date = 09/30/16 Pct Recovery = 84% Analysis Date = 09/30/16 Pct Recovery = 84% Analysis Date = 09/25/16 Pct Recovery = 84% Analysis Date = 09/25/16 Pct Recovery = 84% Analysis Date = 09/20/16 Pct Recovery = 84% Analysis Date = 09/20/16 Pct Recovery = 84% Analysis Date = 09/15/16 Pct Recovery = 84% Analysis Date = 09/15/16 Pct Recovery = 84% Analysis Date = 09/10/16 Pct Recovery = 84% Analysis Date = 09/10/16 Pct Recovery = 84% Analysis Date = 09/06/16 Pct Recovery = 84% Analysis Date = 09/06/16 Pct Recovery = 84% Analysis Date = 09/01/16 Pct Recovery = 84% Analysis Date = 09/01/16 Pct Recovery = 84% Analysis Date = 08/27/16 Pct Recovery = 84% Analysis Date = 08/27/16 Pct Recovery = 84% Analysis Date = 08/22/16 Pct Recovery = 84% Analysis Date = 08/22/16 Pct Recovery = 84% Analysis Date = 08/17/16 Pct Recovery = 84% Analysis Date = 08/17/16 Pct Recovery = 84% Analysis Date = 08/13/16 Pct Recovery = 84% Analysis Date = 08/13/16 Pct Recovery = 84% Analysis Date = 08/08/16 Pct Recovery = 84% Analysis Date = 08/08/16 Pct Recovery = 84% Analysis Date = 08/03/16 Pct Recovery = 84% Analysis Date = 08/03/16 Pct Recovery = 84% Analysis Date = 07/29/16 Pct Recovery = 84% Analysis Date = 07/29/16 Pct Recovery = 84% Analysis Date = 07/24/16 Pct Recovery = 84% Analysis Date = 07/24/16 Pct Recovery = 84% Analysis Date = 07/20/16 Pct Recovery = 84% Analysis Date = 07/20/16 Pct Recovery = 84% Analysis Date = 07/15/16 Pct Recovery = 84% Analysis Date = 07/15/16 Pct Recovery = 84% Analysis Date = 07/10/16 Pct Recovery = 84% Analysis Date = 07/10/16 Pct Recovery = 84% Analysis Date = 07/05/16 Pct Recovery = 85% Analysis Date = 07/05/16 Pct Recovery = 85% Analysis Date = 06/30/16 Pct Recovery = 85% Analysis Date = 06/30/16 Pct Recovery = 85% Analysis Date = 06/26/16 Pct Recovery = 85% Analysis Date = 06/26/16 Pct Recovery = 85% Analysis Date = 06/21/16 Pct Recovery = 85% Analysis Date = 06/21/16 Pct Recovery = 85% Analysis Date = 06/16/16 Pct Recovery = 85% Analysis Date = 06/16/16 Pct Recovery = 85% Analysis Date = 06/11/16 Pct Recovery = 85% Analysis Date = 06/11/16 Pct Recovery = 85% Analysis Date = 06/06/16 Pct Recovery = 85% Analysis Date = 06/06/16 Pct Recovery = 85% Analysis Date = 06/02/16 Pct Recovery = 85% Analysis Date = 06/02/16 Pct Recovery = 85% Analysis Date = 05/28/16 Pct Recovery = 85% Analysis Date = 05/28/16 Pct Recovery = 85% Analysis Date = 05/23/16 Pct Recovery = 85% Analysis Date = 05/23/16 Pct Recovery = 85% Analysis Date = 05/18/16 Pct Recovery = 85% Analysis Date = 05/18/16 Pct Recovery = 85% Analysis Date = 05/13/16 Pct Recovery = 85% Analysis Date = 05/13/16 Pct Recovery = 85% Analysis Date = 05/09/16 Pct Recovery = 85% Analysis Date = 05/09/16 Pct Recovery = 85% Analysis Date = 05/04/16 Pct Recovery = 85% Analysis Date = 05/04/16 Pct Recovery = 85% Analysis Date = 04/29/16 Pct Recovery = 85% Analysis Date = 04/29/16 Pct Recovery = 85% Analysis Date = 04/24/16 Pct Recovery = 85% Analysis Date = 04/24/16 Pct Recovery = 85% Analysis Date = 04/19/16 Pct Recovery = 85% Analysis Date = 04/19/16 Pct Recovery = 85% Analysis Date = 04/15/16 Pct Recovery = 85% Analysis Date = 04/15/16 Pct Recovery = 85% Analysis Date = 04/10/16 Pct Recovery = 85% Analysis Date = 04/10/16 Pct Recovery = 85% Analysis Date = 04/05/16 Pct Recovery = 85% Analysis Date = 04/05/16 Pct Recovery = 85% Analysis Date = 03/31/16 Pct Recovery = 85% Analysis Date = 03/31/16 Pct Recovery = 85% Analysis Date = 03/26/16 Pct Recovery = 85% Analysis Date = 03/26/16 Pct Recovery = 85% Analysis Date = 03/22/16 Pct Recovery = 85% Analysis Date = 03/22/16 Pct Recovery = 85% Analysis Date = 03/17/16 Pct Recovery = 85% Analysis Date = 03/17/16 Pct Recovery = 85% Analysis Date = 03/12/16 Pct Recovery = 85% Analysis Date = 03/12/16 Pct Recovery = 85% Analysis Date = 03/07/16 Pct Recovery = 85% Analysis Date = 03/07/16 Pct Recovery = 85% Analysis Date = 03/02/16 Pct Recovery = 85% Analysis Date = 03/02/16 Pct Recovery = 85% Analysis Date = 02/27/16 Pct Recovery = 85% Analysis Date = 02/27/16 Pct Recovery = 85% Analysis Date = 02/22/16 Pct Recovery = 86% Analysis Date = 02/22/16 Pct Recovery = 86% Analysis Date = 02/17/16 Pct Recovery = 86% Analysis Date = 02/17/16 Pct Recovery = 86% Analysis Date = 02/12/16 Pct Recovery = 86% Analysis Date = 02/12/16 Pct Recovery = 86% Analysis Date = 02/07/16 Pct Recovery = 86% Analysis Date = 02/07/16 Pct Recovery = 86% Analysis Date = 02/03/16 Pct Recovery = 86% Analysis Date = 02/03/16 Pct Recovery = 86% Analysis Date = 01/29/16 Pct Recovery = 86% Analysis Date = 01/29/16 Pct Recovery = 86% Analysis Date = 01/24/16 Pct Recovery = 86% Analysis Date = 01/24/16 Pct Recovery = 86% Analysis Date = 01/19/16 Pct Recovery = 86% Analysis Date = 01/19/16 Pct Recovery = 86% Analysis Date = 01/14/16 Pct Recovery = 86% Analysis Date = 01/14/16 Pct Recovery = 86% Analysis Date = 01/10/16 Pct Recovery = 86% Analysis Date = 01/10/16 Pct Recovery = 86% Analysis Date = 01/05/16 Pct Recovery = 86% Analysis Date = 01/05/16 Pct Recovery = 86% Analysis Date = 12/31/15 Pct Recovery = 86% Analysis Date = 12/31/15 Pct Recovery = 86% Analysis Date = 12/26/15 Pct Recovery = 86% Analysis Date = 12/26/15 Pct Recovery = 86% Analysis Date = 12/21/15 Pct Recovery = 86% Analysis Date = 12/21/15 Pct Recovery = 86% Analysis Date = 12/17/15 Pct Recovery = 86% Analysis Date = 12/17/15 Pct Recovery = 86% Analysis Date = 12/12/15 Pct Recovery = 86% Analysis Date = 12/12/15 Pct Recovery = 86% Analysis Date = 12/07/15 Pct Recovery = 86% Analysis Date = 12/07/15 Pct Recovery = 86% Analysis Date = 12/02/15 Pct Recovery = 87% Analysis Date = 12/02/15 Pct Recovery = 87% Analysis Date = 11/27/15 Pct Recovery = 87% Analysis Date = 11/27/15 Pct Recovery = 87% Analysis Date = 11/23/15 Pct Recovery = 87% Analysis Date = 11/23/15 Pct Recovery = 87% Analysis Date = 11/18/15 Pct Recovery = 87% Analysis Date = 11/18/15 Pct Recovery = 87% Analysis Date = 11/13/15 Pct Recovery = 87% Analysis Date = 11/13/15 Pct Recovery = 87% Analysis Date = 11/08/15 Pct Recovery = 87% Analysis Date = 11/08/15 Pct Recovery = 87% Analysis Date = 11/03/15 Pct Recovery = 87% Analysis Date = 11/03/15 Pct Recovery = 87% Analysis Date = 10/30/15 Pct Recovery = 87% Analysis Date = 10/30/15 Pct Recovery = 87% Analysis Date = 10/25/15 Pct Recovery = 87% Analysis Date = 10/25/15 Pct Recovery = 87% Analysis Date = 10/20/15 Pct Recovery = 87% Analysis Date = 10/20/15 Pct Recovery = 87% Analysis Date = 10/15/15 Pct Recovery = 87% Analysis Date = 10/15/15 Pct Recovery = 87% Analysis Date = 10/10/15 Pct Recovery = 87% Analysis Date = 10/10/15 Pct Recovery = 87% Analysis Date = 10/06/15 Pct Recovery = 88% Analysis Date = 10/06/15 Pct Recovery = 88% Analysis Date = 10/01/15 Pct Recovery = 88% Analysis Date = 10/01/15 Pct Recovery = 88% Analysis Date = 09/26/15 Pct Recovery = 88% Analysis Date = 09/26/15 Pct Recovery = 88% Analysis Date = 09/21/15 Pct Recovery = 88% Analysis Date = 09/21/15 Pct Recovery = 88% Analysis Date = 09/16/15 Pct Recovery = 88% Analysis Date = 09/16/15 Pct Recovery = 88% Analysis Date = 09/12/15 Pct Recovery = 88% Analysis Date = 09/12/15 Pct Recovery = 88% Analysis Date = 09/07/15 Pct Recovery = 88% Analysis Date = 09/07/15 Pct Recovery = 88% Analysis Date = 09/02/15 Pct Recovery = 88% Analysis Date = 09/02/15 Pct Recovery = 88% Analysis Date = 08/28/15 Pct Recovery = 88% Analysis Date = 08/28/15 Pct Recovery = 88% Analysis Date = 08/23/15 Pct Recovery = 89% Analysis Date = 08/23/15 Pct Recovery = 89% Analysis Date = 08/19/15 Pct Recovery = 89% Analysis Date = 08/19/15 Pct Recovery = 89% Analysis Date = 08/14/15 Pct Recovery = 89% Analysis Date = 08/14/15 Pct Recovery = 89% Analysis Date = 08/09/15 Pct Recovery = 89% Analysis Date = 08/09/15 Pct Recovery = 89% Analysis Date = 08/04/15 Pct Recovery = 89% Analysis Date = 08/04/15 Pct Recovery = 89% Analysis Date = 07/30/15 Pct Recovery = 89% Analysis Date = 07/30/15 Pct Recovery = 89% Analysis Date = 07/26/15 Pct Recovery = 89% Analysis Date = 07/26/15 Pct Recovery = 89% Analysis Date = 07/21/15 Pct Recovery = 89% Analysis Date = 07/21/15 Pct Recovery = 89% Analysis Date = 07/16/15 Pct Recovery = 89% Analysis Date = 07/16/15 Pct Recovery = 89% Analysis Date = 07/11/15 Pct Recovery = 90% Analysis Date = 07/11/15 Pct Recovery = 90% Analysis Date = 07/06/15 Pct Recovery = 90% Analysis Date = 07/06/15 Pct Recovery = 90% Analysis Date = 07/02/15 Pct Recovery = 90% Analysis Date = 07/02/15 Pct Recovery = 90% Analysis Date = 06/27/15 Pct Recovery = 90% Analysis Date = 06/27/15 Pct Recovery = 90% Analysis Date = 06/22/15 Pct Recovery = 90% Analysis Date = 06/22/15 Pct Recovery = 90% Analysis Date = 06/17/15 Pct Recovery = 90% Analysis Date = 06/17/15 Pct Recovery = 90% Analysis Date = 06/12/15 Pct Recovery = 90% Analysis Date = 06/12/15 Pct Recovery = 90% Analysis Date = 06/08/15 Pct Recovery = 90% Analysis Date = 06/08/15 Pct Recovery = 90% Analysis Date = 06/03/15 Pct Recovery = 91% Analysis Date = 06/03/15 Pct Recovery = 91% Analysis Date = 05/29/15 Pct Recovery = 91% Analysis Date = 05/29/15 Pct Recovery = 91% Analysis Date = 05/24/15 Pct Recovery = 91% Analysis Date = 05/24/15 Pct Recovery = 91% Analysis Date = 05/19/15 Pct Recovery = 91% Analysis Date = 05/19/15 Pct Recovery = 91% Analysis Date = 05/15/15 Pct Recovery = 91% Analysis Date = 05/15/15 Pct Recovery = 91% Analysis Date = 05/10/15 Pct Recovery = 91% Analysis Date = 05/10/15 Pct Recovery = 91% Analysis Date = 05/05/15 Pct Recovery = 91% Analysis Date = 05/05/15 Pct Recovery = 91% Analysis Date = 04/30/15 Pct Recovery = 92% Analysis Date = 04/30/15 Pct Recovery = 92% Analysis Date = 04/25/15 Pct Recovery = 92% Analysis Date = 04/25/15 Pct Recovery = 92% Analysis Date = 04/21/15 Pct Recovery = 92% Analysis Date = 04/21/15 Pct Recovery = 92% Analysis Date = 04/16/15 Pct Recovery = 92% Analysis Date = 04/16/15 Pct Recovery = 92% Analysis Date = 04/11/15 Pct Recovery = 92% Analysis Date = 04/11/15 Pct Recovery = 92% Analysis Date = 04/06/15 Pct Recovery = 92% Analysis Date = 04/06/15 Pct Recovery = 92% Analysis Date = 04/01/15 Pct Recovery = 93% Analysis Date = 04/01/15 Pct Recovery = 93% Analysis Date = 03/28/15 Pct Recovery = 93% Analysis Date = 03/28/15 Pct Recovery = 93% Analysis Date = 03/23/15 Pct Recovery = 93% Analysis Date = 03/23/15 Pct Recovery = 93% Analysis Date = 03/18/15 Pct Recovery = 93% Analysis Date = 03/18/15 Pct Recovery = 93% Analysis Date = 03/13/15 Pct Recovery = 93% Analysis Date = 03/13/15 Pct Recovery = 93% Analysis Date = 03/08/15 Pct Recovery = 93% Analysis Date = 03/08/15 Pct Recovery = 93% Analysis Date = 03/04/15 Pct Recovery = 93% Analysis Date = 03/04/15 Pct Recovery = 93% Analysis Date = 02/27/15 Pct Recovery = 94% Analysis Date = 02/27/15 Pct Recovery = 94% Analysis Date = 02/22/15 Pct Recovery = 94% Analysis Date = 02/22/15 Pct Recovery = 94% Analysis Date = 02/17/15 Pct Recovery = 94% Analysis Date = 02/17/15 Pct Recovery = 94% Analysis Date = 02/12/15 Pct Recovery = 94% Analysis Date = 02/12/15 Pct Recovery = 94% Analysis Date = 02/08/15 Pct Recovery = 94% Analysis Date = 02/08/15 Pct Recovery = 94% Analysis Date = 02/03/15 Pct Recovery = 94% Analysis Date = 02/03/15 Pct Recovery = 94% Analysis Date = 01/29/15 Pct Recovery = 94% Analysis Date = 01/29/15 Pct Recovery = 94% Analysis Date = 01/24/15 Pct Recovery = 95% Analysis Date = 01/24/15 Pct Recovery = 95% Analysis Date = 01/19/15 Pct Recovery = 95% Analysis Date = 01/19/15 Pct Recovery = 95% Analysis Date = 01/15/15 Pct Recovery = 95% Analysis Date = 01/15/15 Pct Recovery = 95% Analysis Date = 01/10/15 Pct Recovery = 95% Analysis Date = 01/10/15 Pct Recovery = 95% Analysis Date = 01/05/15 Pct Recovery = 95% Analysis Date = 01/05/15 Pct Recovery = 95% Analysis Date = 12/31/14 Pct Recovery = 95% Analysis Date = 12/31/14 Pct Recovery = 95% Analysis Date = 12/26/14 Pct Recovery = 96% Analysis Date = 12/26/14 Pct Recovery = 96% Analysis Date = 12/22/14 Pct Recovery = 96% Analysis Date = 12/22/14 Pct Recovery = 96% Analysis Date = 12/17/14 Pct Recovery = 96% Analysis Date = 12/17/14 Pct Recovery = 96% Analysis Date = 12/12/14 Pct Recovery = 96% Analysis Date = 12/12/14 Pct Recovery = 96% Analysis Date = 12/07/14 Pct Recovery = 96% Analysis Date = 12/07/14 Pct Recovery = 96% Analysis Date = 12/02/14 Pct Recovery = 96% Analysis Date = 12/02/14 Pct Recovery = 96% Analysis Date = 11/28/14 Pct Recovery = 96% Analysis Date = 11/28/14 Pct Recovery = 96% Analysis Date = 11/23/14 Pct Recovery = 96% Analysis Date = 11/23/14 Pct Recovery = 96% Analysis Date = 11/18/14 Pct Recovery = 97% Analysis Date = 11/18/14 Pct Recovery = 97% Analysis Date = 11/13/14 Pct Recovery = 97% Analysis Date = 11/13/14 Pct Recovery = 97% Analysis Date = 11/08/14 Pct Recovery = 97% Analysis Date = 11/08/14 Pct Recovery = 97% Analysis Date = 11/04/14 Pct Recovery = 97% Analysis Date = 11/04/14 Pct Recovery = 97% Analysis Date = 10/30/14 Pct Recovery = 97% Analysis Date = 10/30/14 Pct Recovery = 97% Analysis Date = 10/25/14 Pct Recovery = 97% Analysis Date = 10/25/14 Pct Recovery = 97% Analysis Date = 10/20/14 Pct Recovery = 97% Analysis Date = 10/20/14 Pct Recovery = 97% Analysis Date = 10/15/14 Pct Recovery = 98% Analysis Date = 10/15/14 Pct Recovery = 98% Analysis Date = 10/11/14 Pct Recovery = 98% Analysis Date = 10/11/14 Pct Recovery = 98% Analysis Date = 10/06/14 Pct Recovery = 98% Analysis Date = 10/06/14 Pct Recovery = 98% Analysis Date = 10/01/14 Pct Recovery = 98% Analysis Date = 10/01/14 Pct Recovery = 98% Analysis Date = 09/26/14 Pct Recovery = 98% Analysis Date = 09/26/14 Pct Recovery = 98% Analysis Date = 09/21/14 Pct Recovery = 98% Analysis Date = 09/21/14 Pct Recovery = 98% Analysis Date = 09/17/14 Pct Recovery = 98% Analysis Date = 09/17/14 Pct Recovery = 98% Analysis Date = 09/12/14 Pct Recovery = 99% Analysis Date = 09/12/14 Pct Recovery = 99% Analysis Date = 09/07/14 Pct Recovery = 99% Analysis Date = 09/07/14 Pct Recovery = 99% Analysis Date = 09/02/14 Pct Recovery = 99% Analysis Date = 09/02/14 Pct Recovery = 99% Analysis Date = 08/28/14 Pct Recovery = 99% Analysis Date = 08/28/14 Pct Recovery = 99% Analysis Date = 08/24/14 Pct Recovery = 99% Analysis Date = 08/24/14 Pct Recovery = 99% Analysis Date = 08/19/14 Pct Recovery = 99% Analysis Date = 08/19/14 Pct Recovery = 99% Analysis Date = 08/14/14 Pct Recovery = 99% Analysis Date = 08/14/14 Pct Recovery = 99% Analysis Date = 08/09/14 Pct Recovery = 99% Analysis Date = 08/09/14 Pct Recovery = 99% Analysis Date = 08/04/14 Pct Recovery = 100% Analysis Date = 08/04/14 Pct Recovery = 100% Analysis Date = 07/31/14 Pct Recovery = 100% Analysis Date = 07/31/14 Pct Recovery = 100% Analysis Date = 07/26/14 Pct Recovery = 100% Analysis Date = 07/26/14 Pct Recovery = 100% Analysis Date = 07/21/14 Pct Recovery = 100% Analysis Date = 07/21/14 Pct Recovery = 100% Analysis Date = 07/16/14 Pct Recovery = 100% Analysis Date = 07/16/14 Pct Recovery = 100% Analysis Date = 07/11/14 Pct Recovery = 100% Analysis Date = 07/11/14 Pct Recovery = 100% Analysis Date = 07/07/14 Pct Recovery = 100% Analysis Date = 07/07/14 Pct Recovery = 100% Analysis Date = 07/02/14 Pct Recovery = 101% Analysis Date = 07/02/14 Pct Recovery = 101% Analysis Date = 06/27/14 Pct Recovery = 101% Analysis Date = 06/27/14 Pct Recovery = 101% Analysis Date = 06/22/14 Pct Recovery = 101% Analysis Date = 06/22/14 Pct Recovery = 101% Analysis Date = 06/17/14 Pct Recovery = 101% Analysis Date = 06/17/14 Pct Recovery = 101% Analysis Date = 06/13/14 Pct Recovery = 101% Analysis Date = 06/13/14 Pct Recovery = 101% Analysis Date = 06/08/14 Pct Recovery = 101% Analysis Date = 06/08/14 Pct Recovery = 101% Analysis Date = 06/03/14 Pct Recovery = 101% Analysis Date = 06/03/14 Pct Recovery = 101% Analysis Date = 05/29/14 Pct Recovery = 101% Analysis Date = 05/29/14 Pct Recovery = 101% Analysis Date = 05/24/14 Pct Recovery = 102% Analysis Date = 05/24/14 Pct Recovery = 102% Analysis Date = 05/20/14 Pct Recovery = 102% Analysis Date = 05/20/14 Pct Recovery = 102% Analysis Date = 05/15/14 Pct Recovery = 102% Analysis Date = 05/15/14 Pct Recovery = 102% Analysis Date = 05/10/14 Pct Recovery = 102% Analysis Date = 05/10/14 Pct Recovery = 102% Analysis Date = 05/05/14 Pct Recovery = 102% Analysis Date = 05/05/14 Pct Recovery = 102% Analysis Date = 05/01/14 Pct Recovery = 102% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
ISOPROPYLBENZENE (CUMENE)

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 49 90% 11% 88% 7%
Total 49 90% 11% 88% 7%

Sample Statistics
ISOPROPYLBENZENE (CUMENE)

Characteristic N % % Basis
Plotted 49 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 49 .  
False Negatives 0 0% 0 out of 49
Not Spiked 24 .  
False Positives 0 0% 0 out of 24

BQS OBSP Determination:
M- AND P-XYLENE
METHOD: 4440 , TESTIDCODE: 85795GCM66
Open Data Set

Analysis Date = 12/16/16 SpikeMix = NSI 041816AVOC: 40 µl & ChemService 5082900: 40 µl Pct Recovery = 85% Analysis Date = 07/14/16 SpikeMix = Accu 216041125: 40 µl & NSI 041816AVOC: 40 µl Pct Recovery = 93% Analysis Date = 12/12/16 SpikeMix = Accu 216041125: 40 µl & Crescent 03FF058: 40 µl Pct Recovery = 105% Analysis Date = 08/04/16 SpikeMix = Crescent 03FF058: 40 µl & Supelco LC20141V: 40 µl Pct Recovery = 83% Analysis Date = 08/26/16 SpikeMix = NSI 041816AVOC: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 79% Analysis Date = 11/21/16 SpikeMix = Crescent 03FF058: 25 µl & Supelco LC20141V: 25 µl Pct Recovery = 89% Analysis Date = 06/30/16 SpikeMix = Crescent 03FF058: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 81% Analysis Date = 06/21/16 SpikeMix = Phenova B20160319: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 93% Analysis Date = 05/24/16 SpikeMix = Accu 216041125: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 91% Analysis Date = 03/19/15 SpikeMix = Spex Organics C1140417015: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 81% Analysis Date = 11/14/14 SpikeMix = Crescent 03DD004: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 77% Analysis Date = 06/10/14 SpikeMix = Crescent 03DD004: 20 µl & NSI 032614: 20 µl Pct Recovery = 78% Analysis Date = 04/09/15 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 83% Analysis Date = 08/19/14 SpikeMix = Spex Organics C1140417015: 20 µl & Accu 214031115: 20 µl Pct Recovery = 84% Analysis Date = 07/01/14 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 84% Analysis Date = 05/01/14 SpikeMix = Accu 214031115: 20 µl & NSI 032614: 20 µl Pct Recovery = 76% Analysis Date = 08/15/15 SpikeMix = Supelco LC13545: 25 µl & Crescent 04EE008: 25 µl Pct Recovery = 85% Analysis Date = 07/13/15 SpikeMix = Crescent 04EE008: 25 µl & NSI 050515AVOC: 25 µl Pct Recovery = 80% Analysis Date = 09/29/15 SpikeMix = Accu 215041380: 25 µl & ERA 0406-15-03: 25 µl Pct Recovery = 90% Analysis Date = 10/13/16 SpikeMix = Accu 216041125: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 94% Analysis Date = 10/13/16 SpikeMix = NSI 041816AVOC: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 83% Analysis Date = 07/29/16 SpikeMix = Phenova B20160319: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 85% Analysis Date = 06/10/16 SpikeMix = NSI 041816AVOC: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 91% Analysis Date = 09/28/16 SpikeMix = Crescent 03FF058: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 87% Analysis Date = 09/08/16 SpikeMix = Phenova B20160319: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 83% Analysis Date = 08/20/16 SpikeMix = Accu 216041125: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 92% Analysis Date = 12/18/15 SpikeMix = Supelco LC13545: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 83% Analysis Date = 10/17/15 SpikeMix = Crescent 04EE008: 15 µl & NSI 050515AVOC: 15 µl Pct Recovery = 79% Analysis Date = 05/09/15 SpikeMix = Spex Organics EN150428007: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 86% Analysis Date = 04/02/16 SpikeMix = Supelco LC13545: 15 µl & Accu 215041380: 15 µl Pct Recovery = 85% Analysis Date = 03/04/16 SpikeMix = Accu 215041380: 15 µl & ERA 0406-15-03: 15 µl Pct Recovery = 85% Analysis Date = 06/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Accu 215041380: 15 µl Pct Recovery = 87% Analysis Date = 11/06/14 SpikeMix = Spex Organics C1140417015: 10 µl & Crescent 03DD004: 10 µl Pct Recovery = 85% Analysis Date = 10/04/14 SpikeMix = Crescent 03DD004: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 81% Analysis Date = 07/29/14 SpikeMix = Crescent 03DD004: 10 µl & NSI 032614: 10 µl Pct Recovery = 85% Analysis Date = 01/13/15 SpikeMix = Accu 214031115: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 91% Analysis Date = 09/09/14 SpikeMix = Accu 214031115: 10 µl & NSI 032614: 10 µl Pct Recovery = 106% Analysis Date = 07/23/14 SpikeMix = Spex Organics C1140417015: 10 µl & Accu 214031115: 10 µl Pct Recovery = 101% Analysis Date = 05/13/16 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 88% Analysis Date = 01/27/16 SpikeMix = Crescent 04EE008: 10 µl & NSI 050515AVOC: 10 µl Pct Recovery = 97% Analysis Date = 07/31/15 SpikeMix = Crescent 04EE008: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 80% Analysis Date = 05/09/15 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 91% Analysis Date = 02/18/16 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 84% Analysis Date = 11/20/15 SpikeMix = Accu 215041380: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 94% Analysis Date = 11/12/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 84% Analysis Date = 05/21/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 101% Analysis Date = 12/15/16 Pct Recovery = 90% Analysis Date = 12/11/16 Pct Recovery = 89% Analysis Date = 12/11/16 Pct Recovery = 89% Analysis Date = 12/06/16 Pct Recovery = 89% Analysis Date = 12/06/16 Pct Recovery = 89% Analysis Date = 12/01/16 Pct Recovery = 89% Analysis Date = 12/01/16 Pct Recovery = 89% Analysis Date = 11/26/16 Pct Recovery = 89% Analysis Date = 11/26/16 Pct Recovery = 89% Analysis Date = 11/21/16 Pct Recovery = 89% Analysis Date = 11/21/16 Pct Recovery = 89% Analysis Date = 11/17/16 Pct Recovery = 89% Analysis Date = 11/17/16 Pct Recovery = 89% Analysis Date = 11/12/16 Pct Recovery = 89% Analysis Date = 11/12/16 Pct Recovery = 89% Analysis Date = 11/07/16 Pct Recovery = 89% Analysis Date = 11/07/16 Pct Recovery = 89% Analysis Date = 11/02/16 Pct Recovery = 89% Analysis Date = 11/02/16 Pct Recovery = 89% Analysis Date = 10/28/16 Pct Recovery = 89% Analysis Date = 10/28/16 Pct Recovery = 89% Analysis Date = 10/24/16 Pct Recovery = 89% Analysis Date = 10/24/16 Pct Recovery = 89% Analysis Date = 10/19/16 Pct Recovery = 89% Analysis Date = 10/19/16 Pct Recovery = 89% Analysis Date = 10/14/16 Pct Recovery = 89% Analysis Date = 10/14/16 Pct Recovery = 89% Analysis Date = 10/09/16 Pct Recovery = 89% Analysis Date = 10/09/16 Pct Recovery = 89% Analysis Date = 10/04/16 Pct Recovery = 89% Analysis Date = 10/04/16 Pct Recovery = 89% Analysis Date = 09/30/16 Pct Recovery = 89% Analysis Date = 09/30/16 Pct Recovery = 89% Analysis Date = 09/25/16 Pct Recovery = 89% Analysis Date = 09/25/16 Pct Recovery = 89% Analysis Date = 09/20/16 Pct Recovery = 89% Analysis Date = 09/20/16 Pct Recovery = 89% Analysis Date = 09/15/16 Pct Recovery = 89% Analysis Date = 09/15/16 Pct Recovery = 89% Analysis Date = 09/10/16 Pct Recovery = 88% Analysis Date = 09/10/16 Pct Recovery = 88% Analysis Date = 09/06/16 Pct Recovery = 88% Analysis Date = 09/06/16 Pct Recovery = 88% Analysis Date = 09/01/16 Pct Recovery = 88% Analysis Date = 09/01/16 Pct Recovery = 88% Analysis Date = 08/27/16 Pct Recovery = 88% Analysis Date = 08/27/16 Pct Recovery = 88% Analysis Date = 08/22/16 Pct Recovery = 88% Analysis Date = 08/22/16 Pct Recovery = 88% Analysis Date = 08/17/16 Pct Recovery = 88% Analysis Date = 08/17/16 Pct Recovery = 88% Analysis Date = 08/13/16 Pct Recovery = 88% Analysis Date = 08/13/16 Pct Recovery = 88% Analysis Date = 08/08/16 Pct Recovery = 88% Analysis Date = 08/08/16 Pct Recovery = 88% Analysis Date = 08/03/16 Pct Recovery = 88% Analysis Date = 08/03/16 Pct Recovery = 88% Analysis Date = 07/29/16 Pct Recovery = 88% Analysis Date = 07/29/16 Pct Recovery = 88% Analysis Date = 07/24/16 Pct Recovery = 88% Analysis Date = 07/24/16 Pct Recovery = 88% Analysis Date = 07/20/16 Pct Recovery = 88% Analysis Date = 07/20/16 Pct Recovery = 88% Analysis Date = 07/15/16 Pct Recovery = 88% Analysis Date = 07/15/16 Pct Recovery = 88% Analysis Date = 07/10/16 Pct Recovery = 88% Analysis Date = 07/10/16 Pct Recovery = 88% Analysis Date = 07/05/16 Pct Recovery = 88% Analysis Date = 07/05/16 Pct Recovery = 88% Analysis Date = 06/30/16 Pct Recovery = 88% Analysis Date = 06/30/16 Pct Recovery = 88% Analysis Date = 06/26/16 Pct Recovery = 88% Analysis Date = 06/26/16 Pct Recovery = 88% Analysis Date = 06/21/16 Pct Recovery = 88% Analysis Date = 06/21/16 Pct Recovery = 88% Analysis Date = 06/16/16 Pct Recovery = 88% Analysis Date = 06/16/16 Pct Recovery = 88% Analysis Date = 06/11/16 Pct Recovery = 88% Analysis Date = 06/11/16 Pct Recovery = 88% Analysis Date = 06/06/16 Pct Recovery = 88% Analysis Date = 06/06/16 Pct Recovery = 88% Analysis Date = 06/02/16 Pct Recovery = 88% Analysis Date = 06/02/16 Pct Recovery = 88% Analysis Date = 05/28/16 Pct Recovery = 88% Analysis Date = 05/28/16 Pct Recovery = 88% Analysis Date = 05/23/16 Pct Recovery = 88% Analysis Date = 05/23/16 Pct Recovery = 88% Analysis Date = 05/18/16 Pct Recovery = 88% Analysis Date = 05/18/16 Pct Recovery = 88% Analysis Date = 05/13/16 Pct Recovery = 88% Analysis Date = 05/13/16 Pct Recovery = 88% Analysis Date = 05/09/16 Pct Recovery = 88% Analysis Date = 05/09/16 Pct Recovery = 88% Analysis Date = 05/04/16 Pct Recovery = 88% Analysis Date = 05/04/16 Pct Recovery = 88% Analysis Date = 04/29/16 Pct Recovery = 88% Analysis Date = 04/29/16 Pct Recovery = 88% Analysis Date = 04/24/16 Pct Recovery = 88% Analysis Date = 04/24/16 Pct Recovery = 88% Analysis Date = 04/19/16 Pct Recovery = 88% Analysis Date = 04/19/16 Pct Recovery = 88% Analysis Date = 04/15/16 Pct Recovery = 88% Analysis Date = 04/15/16 Pct Recovery = 88% Analysis Date = 04/10/16 Pct Recovery = 88% Analysis Date = 04/10/16 Pct Recovery = 88% Analysis Date = 04/05/16 Pct Recovery = 88% Analysis Date = 04/05/16 Pct Recovery = 88% Analysis Date = 03/31/16 Pct Recovery = 87% Analysis Date = 03/31/16 Pct Recovery = 87% Analysis Date = 03/26/16 Pct Recovery = 87% Analysis Date = 03/26/16 Pct Recovery = 87% Analysis Date = 03/22/16 Pct Recovery = 87% Analysis Date = 03/22/16 Pct Recovery = 87% Analysis Date = 03/17/16 Pct Recovery = 87% Analysis Date = 03/17/16 Pct Recovery = 87% Analysis Date = 03/12/16 Pct Recovery = 87% Analysis Date = 03/12/16 Pct Recovery = 87% Analysis Date = 03/07/16 Pct Recovery = 87% Analysis Date = 03/07/16 Pct Recovery = 87% Analysis Date = 03/02/16 Pct Recovery = 87% Analysis Date = 03/02/16 Pct Recovery = 87% Analysis Date = 02/27/16 Pct Recovery = 87% Analysis Date = 02/27/16 Pct Recovery = 87% Analysis Date = 02/22/16 Pct Recovery = 87% Analysis Date = 02/22/16 Pct Recovery = 87% Analysis Date = 02/17/16 Pct Recovery = 87% Analysis Date = 02/17/16 Pct Recovery = 87% Analysis Date = 02/12/16 Pct Recovery = 87% Analysis Date = 02/12/16 Pct Recovery = 87% Analysis Date = 02/07/16 Pct Recovery = 87% Analysis Date = 02/07/16 Pct Recovery = 87% Analysis Date = 02/03/16 Pct Recovery = 87% Analysis Date = 02/03/16 Pct Recovery = 87% Analysis Date = 01/29/16 Pct Recovery = 87% Analysis Date = 01/29/16 Pct Recovery = 87% Analysis Date = 01/24/16 Pct Recovery = 87% Analysis Date = 01/24/16 Pct Recovery = 87% Analysis Date = 01/19/16 Pct Recovery = 87% Analysis Date = 01/19/16 Pct Recovery = 87% Analysis Date = 01/14/16 Pct Recovery = 87% Analysis Date = 01/14/16 Pct Recovery = 87% Analysis Date = 01/10/16 Pct Recovery = 87% Analysis Date = 01/10/16 Pct Recovery = 87% Analysis Date = 01/05/16 Pct Recovery = 87% Analysis Date = 01/05/16 Pct Recovery = 87% Analysis Date = 12/31/15 Pct Recovery = 87% Analysis Date = 12/31/15 Pct Recovery = 87% Analysis Date = 12/26/15 Pct Recovery = 87% Analysis Date = 12/26/15 Pct Recovery = 87% Analysis Date = 12/21/15 Pct Recovery = 87% Analysis Date = 12/21/15 Pct Recovery = 87% Analysis Date = 12/17/15 Pct Recovery = 87% Analysis Date = 12/17/15 Pct Recovery = 87% Analysis Date = 12/12/15 Pct Recovery = 87% Analysis Date = 12/12/15 Pct Recovery = 87% Analysis Date = 12/07/15 Pct Recovery = 87% Analysis Date = 12/07/15 Pct Recovery = 87% Analysis Date = 12/02/15 Pct Recovery = 87% Analysis Date = 12/02/15 Pct Recovery = 87% Analysis Date = 11/27/15 Pct Recovery = 87% Analysis Date = 11/27/15 Pct Recovery = 87% Analysis Date = 11/23/15 Pct Recovery = 87% Analysis Date = 11/23/15 Pct Recovery = 87% Analysis Date = 11/18/15 Pct Recovery = 87% Analysis Date = 11/18/15 Pct Recovery = 87% Analysis Date = 11/13/15 Pct Recovery = 87% Analysis Date = 11/13/15 Pct Recovery = 87% Analysis Date = 11/08/15 Pct Recovery = 87% Analysis Date = 11/08/15 Pct Recovery = 87% Analysis Date = 11/03/15 Pct Recovery = 87% Analysis Date = 11/03/15 Pct Recovery = 87% Analysis Date = 10/30/15 Pct Recovery = 87% Analysis Date = 10/30/15 Pct Recovery = 87% Analysis Date = 10/25/15 Pct Recovery = 87% Analysis Date = 10/25/15 Pct Recovery = 87% Analysis Date = 10/20/15 Pct Recovery = 87% Analysis Date = 10/20/15 Pct Recovery = 87% Analysis Date = 10/15/15 Pct Recovery = 87% Analysis Date = 10/15/15 Pct Recovery = 87% Analysis Date = 10/10/15 Pct Recovery = 87% Analysis Date = 10/10/15 Pct Recovery = 87% Analysis Date = 10/06/15 Pct Recovery = 87% Analysis Date = 10/06/15 Pct Recovery = 87% Analysis Date = 10/01/15 Pct Recovery = 87% Analysis Date = 10/01/15 Pct Recovery = 87% Analysis Date = 09/26/15 Pct Recovery = 87% Analysis Date = 09/26/15 Pct Recovery = 87% Analysis Date = 09/21/15 Pct Recovery = 87% Analysis Date = 09/21/15 Pct Recovery = 87% Analysis Date = 09/16/15 Pct Recovery = 87% Analysis Date = 09/16/15 Pct Recovery = 87% Analysis Date = 09/12/15 Pct Recovery = 87% Analysis Date = 09/12/15 Pct Recovery = 87% Analysis Date = 09/07/15 Pct Recovery = 87% Analysis Date = 09/07/15 Pct Recovery = 87% Analysis Date = 09/02/15 Pct Recovery = 87% Analysis Date = 09/02/15 Pct Recovery = 87% Analysis Date = 08/28/15 Pct Recovery = 87% Analysis Date = 08/28/15 Pct Recovery = 87% Analysis Date = 08/23/15 Pct Recovery = 86% Analysis Date = 08/23/15 Pct Recovery = 86% Analysis Date = 08/19/15 Pct Recovery = 86% Analysis Date = 08/19/15 Pct Recovery = 86% Analysis Date = 08/14/15 Pct Recovery = 86% Analysis Date = 08/14/15 Pct Recovery = 86% Analysis Date = 08/09/15 Pct Recovery = 86% Analysis Date = 08/09/15 Pct Recovery = 86% Analysis Date = 08/04/15 Pct Recovery = 86% Analysis Date = 08/04/15 Pct Recovery = 86% Analysis Date = 07/30/15 Pct Recovery = 86% Analysis Date = 07/30/15 Pct Recovery = 86% Analysis Date = 07/26/15 Pct Recovery = 86% Analysis Date = 07/26/15 Pct Recovery = 86% Analysis Date = 07/21/15 Pct Recovery = 86% Analysis Date = 07/21/15 Pct Recovery = 86% Analysis Date = 07/16/15 Pct Recovery = 86% Analysis Date = 07/16/15 Pct Recovery = 86% Analysis Date = 07/11/15 Pct Recovery = 86% Analysis Date = 07/11/15 Pct Recovery = 86% Analysis Date = 07/06/15 Pct Recovery = 86% Analysis Date = 07/06/15 Pct Recovery = 86% Analysis Date = 07/02/15 Pct Recovery = 86% Analysis Date = 07/02/15 Pct Recovery = 86% Analysis Date = 06/27/15 Pct Recovery = 86% Analysis Date = 06/27/15 Pct Recovery = 86% Analysis Date = 06/22/15 Pct Recovery = 86% Analysis Date = 06/22/15 Pct Recovery = 86% Analysis Date = 06/17/15 Pct Recovery = 86% Analysis Date = 06/17/15 Pct Recovery = 86% Analysis Date = 06/12/15 Pct Recovery = 86% Analysis Date = 06/12/15 Pct Recovery = 86% Analysis Date = 06/08/15 Pct Recovery = 86% Analysis Date = 06/08/15 Pct Recovery = 86% Analysis Date = 06/03/15 Pct Recovery = 86% Analysis Date = 06/03/15 Pct Recovery = 86% Analysis Date = 05/29/15 Pct Recovery = 86% Analysis Date = 05/29/15 Pct Recovery = 86% Analysis Date = 05/24/15 Pct Recovery = 86% Analysis Date = 05/24/15 Pct Recovery = 86% Analysis Date = 05/19/15 Pct Recovery = 86% Analysis Date = 05/19/15 Pct Recovery = 86% Analysis Date = 05/15/15 Pct Recovery = 86% Analysis Date = 05/15/15 Pct Recovery = 86% Analysis Date = 05/10/15 Pct Recovery = 86% Analysis Date = 05/10/15 Pct Recovery = 86% Analysis Date = 05/05/15 Pct Recovery = 86% Analysis Date = 05/05/15 Pct Recovery = 86% Analysis Date = 04/30/15 Pct Recovery = 86% Analysis Date = 04/30/15 Pct Recovery = 86% Analysis Date = 04/25/15 Pct Recovery = 86% Analysis Date = 04/25/15 Pct Recovery = 86% Analysis Date = 04/21/15 Pct Recovery = 86% Analysis Date = 04/21/15 Pct Recovery = 86% Analysis Date = 04/16/15 Pct Recovery = 86% Analysis Date = 04/16/15 Pct Recovery = 86% Analysis Date = 04/11/15 Pct Recovery = 86% Analysis Date = 04/11/15 Pct Recovery = 86% Analysis Date = 04/06/15 Pct Recovery = 87% Analysis Date = 04/06/15 Pct Recovery = 87% Analysis Date = 04/01/15 Pct Recovery = 87% Analysis Date = 04/01/15 Pct Recovery = 87% Analysis Date = 03/28/15 Pct Recovery = 87% Analysis Date = 03/28/15 Pct Recovery = 87% Analysis Date = 03/23/15 Pct Recovery = 87% Analysis Date = 03/23/15 Pct Recovery = 87% Analysis Date = 03/18/15 Pct Recovery = 87% Analysis Date = 03/18/15 Pct Recovery = 87% Analysis Date = 03/13/15 Pct Recovery = 87% Analysis Date = 03/13/15 Pct Recovery = 87% Analysis Date = 03/08/15 Pct Recovery = 87% Analysis Date = 03/08/15 Pct Recovery = 87% Analysis Date = 03/04/15 Pct Recovery = 87% Analysis Date = 03/04/15 Pct Recovery = 87% Analysis Date = 02/27/15 Pct Recovery = 87% Analysis Date = 02/27/15 Pct Recovery = 87% Analysis Date = 02/22/15 Pct Recovery = 87% Analysis Date = 02/22/15 Pct Recovery = 87% Analysis Date = 02/17/15 Pct Recovery = 87% Analysis Date = 02/17/15 Pct Recovery = 87% Analysis Date = 02/12/15 Pct Recovery = 87% Analysis Date = 02/12/15 Pct Recovery = 87% Analysis Date = 02/08/15 Pct Recovery = 87% Analysis Date = 02/08/15 Pct Recovery = 87% Analysis Date = 02/03/15 Pct Recovery = 87% Analysis Date = 02/03/15 Pct Recovery = 87% Analysis Date = 01/29/15 Pct Recovery = 87% Analysis Date = 01/29/15 Pct Recovery = 87% Analysis Date = 01/24/15 Pct Recovery = 87% Analysis Date = 01/24/15 Pct Recovery = 87% Analysis Date = 01/19/15 Pct Recovery = 86% Analysis Date = 01/19/15 Pct Recovery = 86% Analysis Date = 01/15/15 Pct Recovery = 86% Analysis Date = 01/15/15 Pct Recovery = 86% Analysis Date = 01/10/15 Pct Recovery = 86% Analysis Date = 01/10/15 Pct Recovery = 86% Analysis Date = 01/05/15 Pct Recovery = 86% Analysis Date = 01/05/15 Pct Recovery = 86% Analysis Date = 12/31/14 Pct Recovery = 86% Analysis Date = 12/31/14 Pct Recovery = 86% Analysis Date = 12/26/14 Pct Recovery = 86% Analysis Date = 12/26/14 Pct Recovery = 86% Analysis Date = 12/22/14 Pct Recovery = 86% Analysis Date = 12/22/14 Pct Recovery = 86% Analysis Date = 12/17/14 Pct Recovery = 86% Analysis Date = 12/17/14 Pct Recovery = 86% Analysis Date = 12/12/14 Pct Recovery = 86% Analysis Date = 12/12/14 Pct Recovery = 86% Analysis Date = 12/07/14 Pct Recovery = 86% Analysis Date = 12/07/14 Pct Recovery = 86% Analysis Date = 12/02/14 Pct Recovery = 86% Analysis Date = 12/02/14 Pct Recovery = 86% Analysis Date = 11/28/14 Pct Recovery = 86% Analysis Date = 11/28/14 Pct Recovery = 86% Analysis Date = 11/23/14 Pct Recovery = 86% Analysis Date = 11/23/14 Pct Recovery = 86% Analysis Date = 11/18/14 Pct Recovery = 86% Analysis Date = 11/18/14 Pct Recovery = 86% Analysis Date = 11/13/14 Pct Recovery = 86% Analysis Date = 11/13/14 Pct Recovery = 86% Analysis Date = 11/08/14 Pct Recovery = 86% Analysis Date = 11/08/14 Pct Recovery = 86% Analysis Date = 11/04/14 Pct Recovery = 86% Analysis Date = 11/04/14 Pct Recovery = 86% Analysis Date = 10/30/14 Pct Recovery = 86% Analysis Date = 10/30/14 Pct Recovery = 86% Analysis Date = 10/25/14 Pct Recovery = 86% Analysis Date = 10/25/14 Pct Recovery = 86% Analysis Date = 10/20/14 Pct Recovery = 86% Analysis Date = 10/20/14 Pct Recovery = 86% Analysis Date = 10/15/14 Pct Recovery = 86% Analysis Date = 10/15/14 Pct Recovery = 86% Analysis Date = 10/11/14 Pct Recovery = 86% Analysis Date = 10/11/14 Pct Recovery = 86% Analysis Date = 10/06/14 Pct Recovery = 86% Analysis Date = 10/06/14 Pct Recovery = 86% Analysis Date = 10/01/14 Pct Recovery = 86% Analysis Date = 10/01/14 Pct Recovery = 86% Analysis Date = 09/26/14 Pct Recovery = 86% Analysis Date = 09/26/14 Pct Recovery = 86% Analysis Date = 09/21/14 Pct Recovery = 86% Analysis Date = 09/21/14 Pct Recovery = 86% Analysis Date = 09/17/14 Pct Recovery = 86% Analysis Date = 09/17/14 Pct Recovery = 86% Analysis Date = 09/12/14 Pct Recovery = 86% Analysis Date = 09/12/14 Pct Recovery = 86% Analysis Date = 09/07/14 Pct Recovery = 86% Analysis Date = 09/07/14 Pct Recovery = 86% Analysis Date = 09/02/14 Pct Recovery = 86% Analysis Date = 09/02/14 Pct Recovery = 86% Analysis Date = 08/28/14 Pct Recovery = 86% Analysis Date = 08/28/14 Pct Recovery = 86% Analysis Date = 08/24/14 Pct Recovery = 86% Analysis Date = 08/24/14 Pct Recovery = 86% Analysis Date = 08/19/14 Pct Recovery = 86% Analysis Date = 08/19/14 Pct Recovery = 86% Analysis Date = 08/14/14 Pct Recovery = 86% Analysis Date = 08/14/14 Pct Recovery = 86% Analysis Date = 08/09/14 Pct Recovery = 86% Analysis Date = 08/09/14 Pct Recovery = 86% Analysis Date = 08/04/14 Pct Recovery = 86% Analysis Date = 08/04/14 Pct Recovery = 86% Analysis Date = 07/31/14 Pct Recovery = 86% Analysis Date = 07/31/14 Pct Recovery = 86% Analysis Date = 07/26/14 Pct Recovery = 86% Analysis Date = 07/26/14 Pct Recovery = 86% Analysis Date = 07/21/14 Pct Recovery = 86% Analysis Date = 07/21/14 Pct Recovery = 86% Analysis Date = 07/16/14 Pct Recovery = 86% Analysis Date = 07/16/14 Pct Recovery = 86% Analysis Date = 07/11/14 Pct Recovery = 86% Analysis Date = 07/11/14 Pct Recovery = 86% Analysis Date = 07/07/14 Pct Recovery = 86% Analysis Date = 07/07/14 Pct Recovery = 86% Analysis Date = 07/02/14 Pct Recovery = 86% Analysis Date = 07/02/14 Pct Recovery = 86% Analysis Date = 06/27/14 Pct Recovery = 86% Analysis Date = 06/27/14 Pct Recovery = 86% Analysis Date = 06/22/14 Pct Recovery = 86% Analysis Date = 06/22/14 Pct Recovery = 86% Analysis Date = 06/17/14 Pct Recovery = 86% Analysis Date = 06/17/14 Pct Recovery = 86% Analysis Date = 06/13/14 Pct Recovery = 85% Analysis Date = 06/13/14 Pct Recovery = 85% Analysis Date = 06/08/14 Pct Recovery = 85% Analysis Date = 06/08/14 Pct Recovery = 85% Analysis Date = 06/03/14 Pct Recovery = 85% Analysis Date = 06/03/14 Pct Recovery = 85% Analysis Date = 05/29/14 Pct Recovery = 85% Analysis Date = 05/29/14 Pct Recovery = 85% Analysis Date = 05/24/14 Pct Recovery = 85% Analysis Date = 05/24/14 Pct Recovery = 85% Analysis Date = 05/20/14 Pct Recovery = 85% Analysis Date = 05/20/14 Pct Recovery = 85% Analysis Date = 05/15/14 Pct Recovery = 85% Analysis Date = 05/15/14 Pct Recovery = 85% Analysis Date = 05/10/14 Pct Recovery = 85% Analysis Date = 05/10/14 Pct Recovery = 85% Analysis Date = 05/05/14 Pct Recovery = 85% Analysis Date = 05/05/14 Pct Recovery = 85% Analysis Date = 05/01/14 Pct Recovery = 85% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
M- AND P-XYLENE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 46 87% 7% 85% 6%
Total 46 87% 7% 85% 6%

Sample Statistics
M- AND P-XYLENE

Characteristic N % % Basis
Plotted 46 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 46 .  
False Negatives 0 0% 0 out of 46
Not Spiked 19 .  
False Positives 0 0% 0 out of 19

BQS OBSP Determination:
METHYL ACRYLATE
METHOD: 4440 , TESTIDCODE: 49991GCM66
Open Data Set

Analysis Date = 08/04/16 SpikeMix = Crescent 03FF058: 40 µl & Supelco LC20141V: 40 µl Pct Recovery = 86% Analysis Date = 07/20/16 SpikeMix = Supelco LC20141V: 40 µl & Accu 216041125: 40 µl Pct Recovery = 105% Analysis Date = 12/16/16 SpikeMix = NSI 041816AVOC: 40 µl & ChemService 5082900: 40 µl Pct Recovery = 103% Analysis Date = 11/21/16 SpikeMix = Crescent 03FF058: 25 µl & Supelco LC20141V: 25 µl Pct Recovery = 92% Analysis Date = 09/08/16 SpikeMix = Supelco LC20141V: 25 µl & Accu 216041125: 25 µl Pct Recovery = 96% Analysis Date = 08/26/16 SpikeMix = NSI 041816AVOC: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 91% Analysis Date = 08/12/16 SpikeMix = ChemService 5082900: 25 µl & Phenova B20160319: 25 µl Pct Recovery = 98% Analysis Date = 06/30/16 SpikeMix = Crescent 03FF058: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 89% Analysis Date = 09/29/15 SpikeMix = Accu 215041380: 25 µl & ERA 0406-15-03: 25 µl Pct Recovery = 92% Analysis Date = 08/15/15 SpikeMix = Supelco LC13545: 25 µl & Crescent 04EE008: 25 µl Pct Recovery = 87% Analysis Date = 07/13/15 SpikeMix = Crescent 04EE008: 25 µl & NSI 050515AVOC: 25 µl Pct Recovery = 86% Analysis Date = 03/19/15 SpikeMix = Spex Organics C1140417015: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 97% Analysis Date = 03/06/15 SpikeMix = ERA 0227-14-06.1A: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 99% Analysis Date = 12/17/14 SpikeMix = Supelco LC06438: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 87% Analysis Date = 11/22/14 SpikeMix = NSI 032614: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 93% Analysis Date = 09/21/14 SpikeMix = Supelco LC06438: 20 µl Pct Recovery = 86% Analysis Date = 08/19/14 SpikeMix = Spex Organics C1140417015: 20 µl & Accu 214031115: 20 µl Pct Recovery = 97% Analysis Date = 08/16/14 SpikeMix = ERA 0227-14-06.1A: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 101% Analysis Date = 06/10/14 SpikeMix = NSI 032614: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 104% Analysis Date = 10/13/16 SpikeMix = NSI 041816AVOC: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 90% Analysis Date = 05/27/16 SpikeMix = Phenova B20160319: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 96% Analysis Date = 11/29/16 SpikeMix = ChemService 5082900: 15 µl & Phenova B20160319: 15 µl Pct Recovery = 100% Analysis Date = 09/28/16 SpikeMix = Crescent 03FF058: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 85% Analysis Date = 06/30/16 SpikeMix = ChemService 5082900: 15 µl & Accu 216041125: 15 µl Pct Recovery = 93% Analysis Date = 06/10/16 SpikeMix = NSI 041816AVOC: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 92% Analysis Date = 04/02/16 SpikeMix = Supelco LC13545: 15 µl & Accu 215041380: 15 µl Pct Recovery = 85% Analysis Date = 03/04/16 SpikeMix = Accu 215041380: 15 µl & ERA 0406-15-03: 15 µl Pct Recovery = 95% Analysis Date = 06/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Accu 215041380: 15 µl Pct Recovery = 84% Analysis Date = 12/18/15 SpikeMix = Supelco LC13545: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 93% Analysis Date = 10/17/15 SpikeMix = Crescent 04EE008: 15 µl & NSI 050515AVOC: 15 µl Pct Recovery = 89% Analysis Date = 05/09/15 SpikeMix = Spex Organics EN150428007: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 92% Analysis Date = 02/18/16 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 94% Analysis Date = 11/20/15 SpikeMix = Accu 215041380: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 91% Analysis Date = 11/12/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 86% Analysis Date = 05/21/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 98% Analysis Date = 05/13/16 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 92% Analysis Date = 01/27/16 SpikeMix = Crescent 04EE008: 10 µl & NSI 050515AVOC: 10 µl Pct Recovery = 83% Analysis Date = 07/31/15 SpikeMix = Crescent 04EE008: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 90% Analysis Date = 05/09/15 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 87% Analysis Date = 11/06/14 SpikeMix = Spex Organics C1140417015: 10 µl & Crescent 03DD004: 10 µl Pct Recovery = 104% Analysis Date = 10/21/14 SpikeMix = ERA 0227-14-06.1A: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 89% Analysis Date = 09/09/14 SpikeMix = NSI 032614: 10 µl & Spex Organics C1140417015: 10 µl Pct Recovery = 101% Analysis Date = 07/23/14 SpikeMix = Spex Organics C1140417015: 10 µl & Accu 214031115: 10 µl Pct Recovery = 94% Analysis Date = 07/11/14 SpikeMix = Spex Organics C1140417015: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 108% Analysis Date = 06/18/14 SpikeMix = Supelco LC06438: 10 µl & Accu 214031115: 10 µl Pct Recovery = 94% Analysis Date = 05/30/14 SpikeMix = NSI 032614: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 92% Analysis Date = 05/03/14 SpikeMix = Crescent 03DD004: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 89% Analysis Date = 12/16/16 Pct Recovery = 96% Analysis Date = 12/11/16 Pct Recovery = 96% Analysis Date = 12/11/16 Pct Recovery = 96% Analysis Date = 12/06/16 Pct Recovery = 96% Analysis Date = 12/06/16 Pct Recovery = 96% Analysis Date = 12/01/16 Pct Recovery = 96% Analysis Date = 12/01/16 Pct Recovery = 96% Analysis Date = 11/26/16 Pct Recovery = 96% Analysis Date = 11/26/16 Pct Recovery = 96% Analysis Date = 11/22/16 Pct Recovery = 95% Analysis Date = 11/22/16 Pct Recovery = 95% Analysis Date = 11/17/16 Pct Recovery = 95% Analysis Date = 11/17/16 Pct Recovery = 95% Analysis Date = 11/12/16 Pct Recovery = 95% Analysis Date = 11/12/16 Pct Recovery = 95% Analysis Date = 11/07/16 Pct Recovery = 95% Analysis Date = 11/07/16 Pct Recovery = 95% Analysis Date = 11/02/16 Pct Recovery = 95% Analysis Date = 11/02/16 Pct Recovery = 95% Analysis Date = 10/29/16 Pct Recovery = 95% Analysis Date = 10/29/16 Pct Recovery = 95% Analysis Date = 10/24/16 Pct Recovery = 95% Analysis Date = 10/24/16 Pct Recovery = 95% Analysis Date = 10/19/16 Pct Recovery = 95% Analysis Date = 10/19/16 Pct Recovery = 95% Analysis Date = 10/14/16 Pct Recovery = 95% Analysis Date = 10/14/16 Pct Recovery = 95% Analysis Date = 10/09/16 Pct Recovery = 95% Analysis Date = 10/09/16 Pct Recovery = 95% Analysis Date = 10/05/16 Pct Recovery = 95% Analysis Date = 10/05/16 Pct Recovery = 95% Analysis Date = 09/30/16 Pct Recovery = 95% Analysis Date = 09/30/16 Pct Recovery = 95% Analysis Date = 09/25/16 Pct Recovery = 94% Analysis Date = 09/25/16 Pct Recovery = 94% Analysis Date = 09/20/16 Pct Recovery = 94% Analysis Date = 09/20/16 Pct Recovery = 94% Analysis Date = 09/15/16 Pct Recovery = 94% Analysis Date = 09/15/16 Pct Recovery = 94% Analysis Date = 09/11/16 Pct Recovery = 94% Analysis Date = 09/11/16 Pct Recovery = 94% Analysis Date = 09/06/16 Pct Recovery = 94% Analysis Date = 09/06/16 Pct Recovery = 94% Analysis Date = 09/01/16 Pct Recovery = 94% Analysis Date = 09/01/16 Pct Recovery = 94% Analysis Date = 08/27/16 Pct Recovery = 94% Analysis Date = 08/27/16 Pct Recovery = 94% Analysis Date = 08/23/16 Pct Recovery = 94% Analysis Date = 08/23/16 Pct Recovery = 94% Analysis Date = 08/18/16 Pct Recovery = 94% Analysis Date = 08/18/16 Pct Recovery = 94% Analysis Date = 08/13/16 Pct Recovery = 94% Analysis Date = 08/13/16 Pct Recovery = 94% Analysis Date = 08/08/16 Pct Recovery = 94% Analysis Date = 08/08/16 Pct Recovery = 94% Analysis Date = 08/03/16 Pct Recovery = 93% Analysis Date = 08/03/16 Pct Recovery = 93% Analysis Date = 07/30/16 Pct Recovery = 93% Analysis Date = 07/30/16 Pct Recovery = 93% Analysis Date = 07/25/16 Pct Recovery = 93% Analysis Date = 07/25/16 Pct Recovery = 93% Analysis Date = 07/20/16 Pct Recovery = 93% Analysis Date = 07/20/16 Pct Recovery = 93% Analysis Date = 07/15/16 Pct Recovery = 93% Analysis Date = 07/15/16 Pct Recovery = 93% Analysis Date = 07/10/16 Pct Recovery = 93% Analysis Date = 07/10/16 Pct Recovery = 93% Analysis Date = 07/06/16 Pct Recovery = 93% Analysis Date = 07/06/16 Pct Recovery = 93% Analysis Date = 07/01/16 Pct Recovery = 93% Analysis Date = 07/01/16 Pct Recovery = 93% Analysis Date = 06/26/16 Pct Recovery = 93% Analysis Date = 06/26/16 Pct Recovery = 93% Analysis Date = 06/21/16 Pct Recovery = 93% Analysis Date = 06/21/16 Pct Recovery = 93% Analysis Date = 06/16/16 Pct Recovery = 93% Analysis Date = 06/16/16 Pct Recovery = 93% Analysis Date = 06/12/16 Pct Recovery = 93% Analysis Date = 06/12/16 Pct Recovery = 93% Analysis Date = 06/07/16 Pct Recovery = 92% Analysis Date = 06/07/16 Pct Recovery = 92% Analysis Date = 06/02/16 Pct Recovery = 92% Analysis Date = 06/02/16 Pct Recovery = 92% Analysis Date = 05/28/16 Pct Recovery = 92% Analysis Date = 05/28/16 Pct Recovery = 92% Analysis Date = 05/24/16 Pct Recovery = 92% Analysis Date = 05/24/16 Pct Recovery = 92% Analysis Date = 05/19/16 Pct Recovery = 92% Analysis Date = 05/19/16 Pct Recovery = 92% Analysis Date = 05/14/16 Pct Recovery = 92% Analysis Date = 05/14/16 Pct Recovery = 92% Analysis Date = 05/09/16 Pct Recovery = 92% Analysis Date = 05/09/16 Pct Recovery = 92% Analysis Date = 05/04/16 Pct Recovery = 92% Analysis Date = 05/04/16 Pct Recovery = 92% Analysis Date = 04/30/16 Pct Recovery = 92% Analysis Date = 04/30/16 Pct Recovery = 92% Analysis Date = 04/25/16 Pct Recovery = 92% Analysis Date = 04/25/16 Pct Recovery = 92% Analysis Date = 04/20/16 Pct Recovery = 92% Analysis Date = 04/20/16 Pct Recovery = 92% Analysis Date = 04/15/16 Pct Recovery = 92% Analysis Date = 04/15/16 Pct Recovery = 92% Analysis Date = 04/10/16 Pct Recovery = 92% Analysis Date = 04/10/16 Pct Recovery = 92% Analysis Date = 04/06/16 Pct Recovery = 92% Analysis Date = 04/06/16 Pct Recovery = 92% Analysis Date = 04/01/16 Pct Recovery = 91% Analysis Date = 04/01/16 Pct Recovery = 91% Analysis Date = 03/27/16 Pct Recovery = 91% Analysis Date = 03/27/16 Pct Recovery = 91% Analysis Date = 03/22/16 Pct Recovery = 91% Analysis Date = 03/22/16 Pct Recovery = 91% Analysis Date = 03/17/16 Pct Recovery = 91% Analysis Date = 03/17/16 Pct Recovery = 91% Analysis Date = 03/13/16 Pct Recovery = 91% Analysis Date = 03/13/16 Pct Recovery = 91% Analysis Date = 03/08/16 Pct Recovery = 91% Analysis Date = 03/08/16 Pct Recovery = 91% Analysis Date = 03/03/16 Pct Recovery = 91% Analysis Date = 03/03/16 Pct Recovery = 91% Analysis Date = 02/27/16 Pct Recovery = 91% Analysis Date = 02/27/16 Pct Recovery = 91% Analysis Date = 02/23/16 Pct Recovery = 91% Analysis Date = 02/23/16 Pct Recovery = 91% Analysis Date = 02/18/16 Pct Recovery = 91% Analysis Date = 02/18/16 Pct Recovery = 91% Analysis Date = 02/13/16 Pct Recovery = 91% Analysis Date = 02/13/16 Pct Recovery = 91% Analysis Date = 02/08/16 Pct Recovery = 91% Analysis Date = 02/08/16 Pct Recovery = 91% Analysis Date = 02/03/16 Pct Recovery = 91% Analysis Date = 02/03/16 Pct Recovery = 91% Analysis Date = 01/30/16 Pct Recovery = 91% Analysis Date = 01/30/16 Pct Recovery = 91% Analysis Date = 01/25/16 Pct Recovery = 91% Analysis Date = 01/25/16 Pct Recovery = 91% Analysis Date = 01/20/16 Pct Recovery = 91% Analysis Date = 01/20/16 Pct Recovery = 91% Analysis Date = 01/15/16 Pct Recovery = 91% Analysis Date = 01/15/16 Pct Recovery = 91% Analysis Date = 01/10/16 Pct Recovery = 90% Analysis Date = 01/10/16 Pct Recovery = 90% Analysis Date = 01/06/16 Pct Recovery = 90% Analysis Date = 01/06/16 Pct Recovery = 90% Analysis Date = 01/01/16 Pct Recovery = 90% Analysis Date = 01/01/16 Pct Recovery = 90% Analysis Date = 12/27/15 Pct Recovery = 90% Analysis Date = 12/27/15 Pct Recovery = 90% Analysis Date = 12/22/15 Pct Recovery = 90% Analysis Date = 12/22/15 Pct Recovery = 90% Analysis Date = 12/17/15 Pct Recovery = 90% Analysis Date = 12/17/15 Pct Recovery = 90% Analysis Date = 12/13/15 Pct Recovery = 90% Analysis Date = 12/13/15 Pct Recovery = 90% Analysis Date = 12/08/15 Pct Recovery = 90% Analysis Date = 12/08/15 Pct Recovery = 90% Analysis Date = 12/03/15 Pct Recovery = 90% Analysis Date = 12/03/15 Pct Recovery = 90% Analysis Date = 11/28/15 Pct Recovery = 90% Analysis Date = 11/28/15 Pct Recovery = 90% Analysis Date = 11/24/15 Pct Recovery = 90% Analysis Date = 11/24/15 Pct Recovery = 90% Analysis Date = 11/19/15 Pct Recovery = 90% Analysis Date = 11/19/15 Pct Recovery = 90% Analysis Date = 11/14/15 Pct Recovery = 90% Analysis Date = 11/14/15 Pct Recovery = 90% Analysis Date = 11/09/15 Pct Recovery = 90% Analysis Date = 11/09/15 Pct Recovery = 90% Analysis Date = 11/04/15 Pct Recovery = 90% Analysis Date = 11/04/15 Pct Recovery = 90% Analysis Date = 10/31/15 Pct Recovery = 90% Analysis Date = 10/31/15 Pct Recovery = 90% Analysis Date = 10/26/15 Pct Recovery = 90% Analysis Date = 10/26/15 Pct Recovery = 90% Analysis Date = 10/21/15 Pct Recovery = 90% Analysis Date = 10/21/15 Pct Recovery = 90% Analysis Date = 10/16/15 Pct Recovery = 90% Analysis Date = 10/16/15 Pct Recovery = 90% Analysis Date = 10/11/15 Pct Recovery = 90% Analysis Date = 10/11/15 Pct Recovery = 90% Analysis Date = 10/07/15 Pct Recovery = 90% Analysis Date = 10/07/15 Pct Recovery = 90% Analysis Date = 10/02/15 Pct Recovery = 90% Analysis Date = 10/02/15 Pct Recovery = 90% Analysis Date = 09/27/15 Pct Recovery = 90% Analysis Date = 09/27/15 Pct Recovery = 90% Analysis Date = 09/22/15 Pct Recovery = 90% Analysis Date = 09/22/15 Pct Recovery = 90% Analysis Date = 09/17/15 Pct Recovery = 90% Analysis Date = 09/17/15 Pct Recovery = 90% Analysis Date = 09/13/15 Pct Recovery = 90% Analysis Date = 09/13/15 Pct Recovery = 90% Analysis Date = 09/08/15 Pct Recovery = 90% Analysis Date = 09/08/15 Pct Recovery = 90% Analysis Date = 09/03/15 Pct Recovery = 90% Analysis Date = 09/03/15 Pct Recovery = 90% Analysis Date = 08/29/15 Pct Recovery = 90% Analysis Date = 08/29/15 Pct Recovery = 90% Analysis Date = 08/25/15 Pct Recovery = 90% Analysis Date = 08/25/15 Pct Recovery = 90% Analysis Date = 08/20/15 Pct Recovery = 90% Analysis Date = 08/20/15 Pct Recovery = 90% Analysis Date = 08/15/15 Pct Recovery = 90% Analysis Date = 08/15/15 Pct Recovery = 90% Analysis Date = 08/10/15 Pct Recovery = 90% Analysis Date = 08/10/15 Pct Recovery = 90% Analysis Date = 08/05/15 Pct Recovery = 91% Analysis Date = 08/05/15 Pct Recovery = 91% Analysis Date = 08/01/15 Pct Recovery = 91% Analysis Date = 08/01/15 Pct Recovery = 91% Analysis Date = 07/27/15 Pct Recovery = 91% Analysis Date = 07/27/15 Pct Recovery = 91% Analysis Date = 07/22/15 Pct Recovery = 91% Analysis Date = 07/22/15 Pct Recovery = 91% Analysis Date = 07/17/15 Pct Recovery = 91% Analysis Date = 07/17/15 Pct Recovery = 91% Analysis Date = 07/12/15 Pct Recovery = 91% Analysis Date = 07/12/15 Pct Recovery = 91% Analysis Date = 07/08/15 Pct Recovery = 91% Analysis Date = 07/08/15 Pct Recovery = 91% Analysis Date = 07/03/15 Pct Recovery = 91% Analysis Date = 07/03/15 Pct Recovery = 91% Analysis Date = 06/28/15 Pct Recovery = 91% Analysis Date = 06/28/15 Pct Recovery = 91% Analysis Date = 06/23/15 Pct Recovery = 91% Analysis Date = 06/23/15 Pct Recovery = 91% Analysis Date = 06/18/15 Pct Recovery = 91% Analysis Date = 06/18/15 Pct Recovery = 91% Analysis Date = 06/14/15 Pct Recovery = 91% Analysis Date = 06/14/15 Pct Recovery = 91% Analysis Date = 06/09/15 Pct Recovery = 91% Analysis Date = 06/09/15 Pct Recovery = 91% Analysis Date = 06/04/15 Pct Recovery = 91% Analysis Date = 06/04/15 Pct Recovery = 91% Analysis Date = 05/30/15 Pct Recovery = 91% Analysis Date = 05/30/15 Pct Recovery = 91% Analysis Date = 05/25/15 Pct Recovery = 91% Analysis Date = 05/25/15 Pct Recovery = 91% Analysis Date = 05/21/15 Pct Recovery = 91% Analysis Date = 05/21/15 Pct Recovery = 91% Analysis Date = 05/16/15 Pct Recovery = 91% Analysis Date = 05/16/15 Pct Recovery = 91% Analysis Date = 05/11/15 Pct Recovery = 91% Analysis Date = 05/11/15 Pct Recovery = 91% Analysis Date = 05/06/15 Pct Recovery = 92% Analysis Date = 05/06/15 Pct Recovery = 92% Analysis Date = 05/02/15 Pct Recovery = 92% Analysis Date = 05/02/15 Pct Recovery = 92% Analysis Date = 04/27/15 Pct Recovery = 92% Analysis Date = 04/27/15 Pct Recovery = 92% Analysis Date = 04/22/15 Pct Recovery = 92% Analysis Date = 04/22/15 Pct Recovery = 92% Analysis Date = 04/17/15 Pct Recovery = 92% Analysis Date = 04/17/15 Pct Recovery = 92% Analysis Date = 04/12/15 Pct Recovery = 92% Analysis Date = 04/12/15 Pct Recovery = 92% Analysis Date = 04/08/15 Pct Recovery = 92% Analysis Date = 04/08/15 Pct Recovery = 92% Analysis Date = 04/03/15 Pct Recovery = 92% Analysis Date = 04/03/15 Pct Recovery = 92% Analysis Date = 03/29/15 Pct Recovery = 92% Analysis Date = 03/29/15 Pct Recovery = 92% Analysis Date = 03/24/15 Pct Recovery = 92% Analysis Date = 03/24/15 Pct Recovery = 92% Analysis Date = 03/19/15 Pct Recovery = 92% Analysis Date = 03/19/15 Pct Recovery = 92% Analysis Date = 03/15/15 Pct Recovery = 92% Analysis Date = 03/15/15 Pct Recovery = 92% Analysis Date = 03/10/15 Pct Recovery = 92% Analysis Date = 03/10/15 Pct Recovery = 92% Analysis Date = 03/05/15 Pct Recovery = 93% Analysis Date = 03/05/15 Pct Recovery = 93% Analysis Date = 02/28/15 Pct Recovery = 93% Analysis Date = 02/28/15 Pct Recovery = 93% Analysis Date = 02/23/15 Pct Recovery = 93% Analysis Date = 02/23/15 Pct Recovery = 93% Analysis Date = 02/19/15 Pct Recovery = 93% Analysis Date = 02/19/15 Pct Recovery = 93% Analysis Date = 02/14/15 Pct Recovery = 93% Analysis Date = 02/14/15 Pct Recovery = 93% Analysis Date = 02/09/15 Pct Recovery = 93% Analysis Date = 02/09/15 Pct Recovery = 93% Analysis Date = 02/04/15 Pct Recovery = 93% Analysis Date = 02/04/15 Pct Recovery = 93% Analysis Date = 01/31/15 Pct Recovery = 93% Analysis Date = 01/31/15 Pct Recovery = 93% Analysis Date = 01/26/15 Pct Recovery = 93% Analysis Date = 01/26/15 Pct Recovery = 93% Analysis Date = 01/21/15 Pct Recovery = 93% Analysis Date = 01/21/15 Pct Recovery = 93% Analysis Date = 01/16/15 Pct Recovery = 93% Analysis Date = 01/16/15 Pct Recovery = 93% Analysis Date = 01/11/15 Pct Recovery = 93% Analysis Date = 01/11/15 Pct Recovery = 93% Analysis Date = 01/07/15 Pct Recovery = 94% Analysis Date = 01/07/15 Pct Recovery = 94% Analysis Date = 01/02/15 Pct Recovery = 94% Analysis Date = 01/02/15 Pct Recovery = 94% Analysis Date = 12/28/14 Pct Recovery = 94% Analysis Date = 12/28/14 Pct Recovery = 94% Analysis Date = 12/23/14 Pct Recovery = 94% Analysis Date = 12/23/14 Pct Recovery = 94% Analysis Date = 12/18/14 Pct Recovery = 94% Analysis Date = 12/18/14 Pct Recovery = 94% Analysis Date = 12/14/14 Pct Recovery = 94% Analysis Date = 12/14/14 Pct Recovery = 94% Analysis Date = 12/09/14 Pct Recovery = 94% Analysis Date = 12/09/14 Pct Recovery = 94% Analysis Date = 12/04/14 Pct Recovery = 94% Analysis Date = 12/04/14 Pct Recovery = 94% Analysis Date = 11/29/14 Pct Recovery = 94% Analysis Date = 11/29/14 Pct Recovery = 94% Analysis Date = 11/24/14 Pct Recovery = 94% Analysis Date = 11/24/14 Pct Recovery = 94% Analysis Date = 11/20/14 Pct Recovery = 94% Analysis Date = 11/20/14 Pct Recovery = 94% Analysis Date = 11/15/14 Pct Recovery = 95% Analysis Date = 11/15/14 Pct Recovery = 95% Analysis Date = 11/10/14 Pct Recovery = 95% Analysis Date = 11/10/14 Pct Recovery = 95% Analysis Date = 11/05/14 Pct Recovery = 95% Analysis Date = 11/05/14 Pct Recovery = 95% Analysis Date = 11/01/14 Pct Recovery = 95% Analysis Date = 11/01/14 Pct Recovery = 95% Analysis Date = 10/27/14 Pct Recovery = 95% Analysis Date = 10/27/14 Pct Recovery = 95% Analysis Date = 10/22/14 Pct Recovery = 95% Analysis Date = 10/22/14 Pct Recovery = 95% Analysis Date = 10/17/14 Pct Recovery = 95% Analysis Date = 10/17/14 Pct Recovery = 95% Analysis Date = 10/12/14 Pct Recovery = 95% Analysis Date = 10/12/14 Pct Recovery = 95% Analysis Date = 10/08/14 Pct Recovery = 95% Analysis Date = 10/08/14 Pct Recovery = 95% Analysis Date = 10/03/14 Pct Recovery = 95% Analysis Date = 10/03/14 Pct Recovery = 95% Analysis Date = 09/28/14 Pct Recovery = 95% Analysis Date = 09/28/14 Pct Recovery = 95% Analysis Date = 09/23/14 Pct Recovery = 95% Analysis Date = 09/23/14 Pct Recovery = 95% Analysis Date = 09/18/14 Pct Recovery = 95% Analysis Date = 09/18/14 Pct Recovery = 95% Analysis Date = 09/14/14 Pct Recovery = 96% Analysis Date = 09/14/14 Pct Recovery = 96% Analysis Date = 09/09/14 Pct Recovery = 96% Analysis Date = 09/09/14 Pct Recovery = 96% Analysis Date = 09/04/14 Pct Recovery = 96% Analysis Date = 09/04/14 Pct Recovery = 96% Analysis Date = 08/30/14 Pct Recovery = 96% Analysis Date = 08/30/14 Pct Recovery = 96% Analysis Date = 08/25/14 Pct Recovery = 96% Analysis Date = 08/25/14 Pct Recovery = 96% Analysis Date = 08/21/14 Pct Recovery = 96% Analysis Date = 08/21/14 Pct Recovery = 96% Analysis Date = 08/16/14 Pct Recovery = 96% Analysis Date = 08/16/14 Pct Recovery = 96% Analysis Date = 08/11/14 Pct Recovery = 96% Analysis Date = 08/11/14 Pct Recovery = 96% Analysis Date = 08/06/14 Pct Recovery = 96% Analysis Date = 08/06/14 Pct Recovery = 96% Analysis Date = 08/02/14 Pct Recovery = 96% Analysis Date = 08/02/14 Pct Recovery = 96% Analysis Date = 07/28/14 Pct Recovery = 96% Analysis Date = 07/28/14 Pct Recovery = 96% Analysis Date = 07/23/14 Pct Recovery = 96% Analysis Date = 07/23/14 Pct Recovery = 96% Analysis Date = 07/18/14 Pct Recovery = 96% Analysis Date = 07/18/14 Pct Recovery = 96% Analysis Date = 07/13/14 Pct Recovery = 96% Analysis Date = 07/13/14 Pct Recovery = 96% Analysis Date = 07/09/14 Pct Recovery = 96% Analysis Date = 07/09/14 Pct Recovery = 96% Analysis Date = 07/04/14 Pct Recovery = 97% Analysis Date = 07/04/14 Pct Recovery = 97% Analysis Date = 06/29/14 Pct Recovery = 97% Analysis Date = 06/29/14 Pct Recovery = 97% Analysis Date = 06/24/14 Pct Recovery = 97% Analysis Date = 06/24/14 Pct Recovery = 97% Analysis Date = 06/19/14 Pct Recovery = 97% Analysis Date = 06/19/14 Pct Recovery = 97% Analysis Date = 06/15/14 Pct Recovery = 97% Analysis Date = 06/15/14 Pct Recovery = 97% Analysis Date = 06/10/14 Pct Recovery = 97% Analysis Date = 06/10/14 Pct Recovery = 97% Analysis Date = 06/05/14 Pct Recovery = 97% Analysis Date = 06/05/14 Pct Recovery = 97% Analysis Date = 05/31/14 Pct Recovery = 97% Analysis Date = 05/31/14 Pct Recovery = 97% Analysis Date = 05/26/14 Pct Recovery = 97% Analysis Date = 05/26/14 Pct Recovery = 97% Analysis Date = 05/22/14 Pct Recovery = 97% Analysis Date = 05/22/14 Pct Recovery = 97% Analysis Date = 05/17/14 Pct Recovery = 97% Analysis Date = 05/17/14 Pct Recovery = 97% Analysis Date = 05/12/14 Pct Recovery = 97% Analysis Date = 05/12/14 Pct Recovery = 97% Analysis Date = 05/07/14 Pct Recovery = 97% Analysis Date = 05/07/14 Pct Recovery = 97% Analysis Date = 05/03/14 Pct Recovery = 97% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
METHYL ACRYLATE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 47 93% 6% 92% 6%
Total 47 93% 6% 92% 6%

Sample Statistics
METHYL ACRYLATE

Characteristic N % % Basis
Plotted 47 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 47 .  
False Negatives 0 0% 0 out of 47
Not Spiked 26 .  
False Positives 0 0% 0 out of 26

BQS OBSP Determination:
METHYL ACRYLONITRILE
METHOD: 4440 , TESTIDCODE: 81593GCM66
Open Data Set

Analysis Date = 12/16/16 SpikeMix = NSI 041816AVOC: 40 µl & ChemService 5082900: 40 µl Pct Recovery = 104% Analysis Date = 07/14/16 SpikeMix = Accu 216041125: 40 µl & NSI 041816AVOC: 40 µl Pct Recovery = 101% Analysis Date = 12/12/16 SpikeMix = Accu 216041125: 40 µl & Crescent 03FF058: 40 µl Pct Recovery = 105% Analysis Date = 08/04/16 SpikeMix = Crescent 03FF058: 40 µl & Supelco LC20141V: 40 µl Pct Recovery = 92% Analysis Date = 08/26/16 SpikeMix = NSI 041816AVOC: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 100% Analysis Date = 11/21/16 SpikeMix = Crescent 03FF058: 25 µl & Supelco LC20141V: 25 µl Pct Recovery = 93% Analysis Date = 06/30/16 SpikeMix = Crescent 03FF058: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 95% Analysis Date = 06/21/16 SpikeMix = Phenova B20160319: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 103% Analysis Date = 05/24/16 SpikeMix = Accu 216041125: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 95% Analysis Date = 09/29/15 SpikeMix = Accu 215041380: 25 µl & ERA 0406-15-03: 25 µl Pct Recovery = 93% Analysis Date = 08/15/15 SpikeMix = Supelco LC13545: 25 µl & Crescent 04EE008: 25 µl Pct Recovery = 90% Analysis Date = 07/13/15 SpikeMix = Crescent 04EE008: 25 µl & NSI 050515AVOC: 25 µl Pct Recovery = 95% Analysis Date = 04/09/15 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 94% Analysis Date = 08/19/14 SpikeMix = Spex Organics C1140417015: 20 µl & Accu 214031115: 20 µl Pct Recovery = 107% Analysis Date = 07/01/14 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 104% Analysis Date = 05/01/14 SpikeMix = Accu 214031115: 20 µl & NSI 032614: 20 µl Pct Recovery = 91% Analysis Date = 03/19/15 SpikeMix = Spex Organics C1140417015: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 100% Analysis Date = 12/17/14 SpikeMix = Supelco LC06438: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 103% Analysis Date = 11/14/14 SpikeMix = Crescent 03DD004: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 98% Analysis Date = 06/10/14 SpikeMix = Crescent 03DD004: 20 µl & NSI 032614: 20 µl Pct Recovery = 99% Analysis Date = 10/13/16 SpikeMix = Accu 216041125: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 117% Analysis Date = 10/13/16 SpikeMix = NSI 041816AVOC: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 102% Analysis Date = 07/29/16 SpikeMix = Phenova B20160319: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 94% Analysis Date = 06/10/16 SpikeMix = NSI 041816AVOC: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 107% Analysis Date = 09/28/16 SpikeMix = Crescent 03FF058: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 103% Analysis Date = 09/08/16 SpikeMix = Phenova B20160319: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 90% Analysis Date = 08/20/16 SpikeMix = Accu 216041125: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 99% Analysis Date = 04/02/16 SpikeMix = Supelco LC13545: 15 µl & Accu 215041380: 15 µl Pct Recovery = 106% Analysis Date = 03/04/16 SpikeMix = Accu 215041380: 15 µl & ERA 0406-15-03: 15 µl Pct Recovery = 97% Analysis Date = 06/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Accu 215041380: 15 µl Pct Recovery = 93% Analysis Date = 12/18/15 SpikeMix = Supelco LC13545: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 112% Analysis Date = 10/17/15 SpikeMix = Crescent 04EE008: 15 µl & NSI 050515AVOC: 15 µl Pct Recovery = 106% Analysis Date = 05/09/15 SpikeMix = Spex Organics EN150428007: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 114% Analysis Date = 01/13/15 SpikeMix = Accu 214031115: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 100% Analysis Date = 09/09/14 SpikeMix = Accu 214031115: 10 µl & NSI 032614: 10 µl Pct Recovery = 96% Analysis Date = 07/23/14 SpikeMix = Spex Organics C1140417015: 10 µl & Accu 214031115: 10 µl Pct Recovery = 112% Analysis Date = 06/18/14 SpikeMix = Supelco LC06438: 10 µl & Accu 214031115: 10 µl Pct Recovery = 108% Analysis Date = 11/06/14 SpikeMix = Spex Organics C1140417015: 10 µl & Crescent 03DD004: 10 µl Pct Recovery = 102% Analysis Date = 10/04/14 SpikeMix = Crescent 03DD004: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 93% Analysis Date = 07/29/14 SpikeMix = Crescent 03DD004: 10 µl & NSI 032614: 10 µl Pct Recovery = 108% Analysis Date = 05/03/14 SpikeMix = Crescent 03DD004: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 110% Analysis Date = 02/18/16 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 93% Analysis Date = 11/20/15 SpikeMix = Accu 215041380: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 99% Analysis Date = 11/12/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 97% Analysis Date = 05/21/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 102% Analysis Date = 05/13/16 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 112% Analysis Date = 01/27/16 SpikeMix = Crescent 04EE008: 10 µl & NSI 050515AVOC: 10 µl Pct Recovery = 90% Analysis Date = 08/07/15 SpikeMix = Crescent 04EE008: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 97% Analysis Date = 05/09/15 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 109% Analysis Date = 12/15/16 Pct Recovery = 102% Analysis Date = 12/11/16 Pct Recovery = 102% Analysis Date = 12/11/16 Pct Recovery = 102% Analysis Date = 12/06/16 Pct Recovery = 102% Analysis Date = 12/06/16 Pct Recovery = 102% Analysis Date = 12/01/16 Pct Recovery = 102% Analysis Date = 12/01/16 Pct Recovery = 102% Analysis Date = 11/26/16 Pct Recovery = 101% Analysis Date = 11/26/16 Pct Recovery = 101% Analysis Date = 11/21/16 Pct Recovery = 101% Analysis Date = 11/21/16 Pct Recovery = 101% Analysis Date = 11/17/16 Pct Recovery = 101% Analysis Date = 11/17/16 Pct Recovery = 101% Analysis Date = 11/12/16 Pct Recovery = 101% Analysis Date = 11/12/16 Pct Recovery = 101% Analysis Date = 11/07/16 Pct Recovery = 101% Analysis Date = 11/07/16 Pct Recovery = 101% Analysis Date = 11/02/16 Pct Recovery = 101% Analysis Date = 11/02/16 Pct Recovery = 101% Analysis Date = 10/28/16 Pct Recovery = 101% Analysis Date = 10/28/16 Pct Recovery = 101% Analysis Date = 10/24/16 Pct Recovery = 101% Analysis Date = 10/24/16 Pct Recovery = 101% Analysis Date = 10/19/16 Pct Recovery = 101% Analysis Date = 10/19/16 Pct Recovery = 101% Analysis Date = 10/14/16 Pct Recovery = 101% Analysis Date = 10/14/16 Pct Recovery = 101% Analysis Date = 10/09/16 Pct Recovery = 101% Analysis Date = 10/09/16 Pct Recovery = 101% Analysis Date = 10/04/16 Pct Recovery = 101% Analysis Date = 10/04/16 Pct Recovery = 101% Analysis Date = 09/30/16 Pct Recovery = 101% Analysis Date = 09/30/16 Pct Recovery = 101% Analysis Date = 09/25/16 Pct Recovery = 101% Analysis Date = 09/25/16 Pct Recovery = 101% Analysis Date = 09/20/16 Pct Recovery = 101% Analysis Date = 09/20/16 Pct Recovery = 101% Analysis Date = 09/15/16 Pct Recovery = 101% Analysis Date = 09/15/16 Pct Recovery = 101% Analysis Date = 09/10/16 Pct Recovery = 101% Analysis Date = 09/10/16 Pct Recovery = 101% Analysis Date = 09/06/16 Pct Recovery = 101% Analysis Date = 09/06/16 Pct Recovery = 101% Analysis Date = 09/01/16 Pct Recovery = 101% Analysis Date = 09/01/16 Pct Recovery = 101% Analysis Date = 08/27/16 Pct Recovery = 101% Analysis Date = 08/27/16 Pct Recovery = 101% Analysis Date = 08/22/16 Pct Recovery = 101% Analysis Date = 08/22/16 Pct Recovery = 101% Analysis Date = 08/17/16 Pct Recovery = 101% Analysis Date = 08/17/16 Pct Recovery = 101% Analysis Date = 08/13/16 Pct Recovery = 101% Analysis Date = 08/13/16 Pct Recovery = 101% Analysis Date = 08/08/16 Pct Recovery = 101% Analysis Date = 08/08/16 Pct Recovery = 101% Analysis Date = 08/03/16 Pct Recovery = 101% Analysis Date = 08/03/16 Pct Recovery = 101% Analysis Date = 07/29/16 Pct Recovery = 101% Analysis Date = 07/29/16 Pct Recovery = 101% Analysis Date = 07/24/16 Pct Recovery = 100% Analysis Date = 07/24/16 Pct Recovery = 100% Analysis Date = 07/20/16 Pct Recovery = 100% Analysis Date = 07/20/16 Pct Recovery = 100% Analysis Date = 07/15/16 Pct Recovery = 100% Analysis Date = 07/15/16 Pct Recovery = 100% Analysis Date = 07/10/16 Pct Recovery = 100% Analysis Date = 07/10/16 Pct Recovery = 100% Analysis Date = 07/05/16 Pct Recovery = 100% Analysis Date = 07/05/16 Pct Recovery = 100% Analysis Date = 06/30/16 Pct Recovery = 100% Analysis Date = 06/30/16 Pct Recovery = 100% Analysis Date = 06/26/16 Pct Recovery = 100% Analysis Date = 06/26/16 Pct Recovery = 100% Analysis Date = 06/21/16 Pct Recovery = 100% Analysis Date = 06/21/16 Pct Recovery = 100% Analysis Date = 06/16/16 Pct Recovery = 100% Analysis Date = 06/16/16 Pct Recovery = 100% Analysis Date = 06/11/16 Pct Recovery = 100% Analysis Date = 06/11/16 Pct Recovery = 100% Analysis Date = 06/06/16 Pct Recovery = 100% Analysis Date = 06/06/16 Pct Recovery = 100% Analysis Date = 06/02/16 Pct Recovery = 100% Analysis Date = 06/02/16 Pct Recovery = 100% Analysis Date = 05/28/16 Pct Recovery = 100% Analysis Date = 05/28/16 Pct Recovery = 100% Analysis Date = 05/23/16 Pct Recovery = 100% Analysis Date = 05/23/16 Pct Recovery = 100% Analysis Date = 05/18/16 Pct Recovery = 100% Analysis Date = 05/18/16 Pct Recovery = 100% Analysis Date = 05/13/16 Pct Recovery = 100% Analysis Date = 05/13/16 Pct Recovery = 100% Analysis Date = 05/09/16 Pct Recovery = 100% Analysis Date = 05/09/16 Pct Recovery = 100% Analysis Date = 05/04/16 Pct Recovery = 100% Analysis Date = 05/04/16 Pct Recovery = 100% Analysis Date = 04/29/16 Pct Recovery = 100% Analysis Date = 04/29/16 Pct Recovery = 100% Analysis Date = 04/24/16 Pct Recovery = 100% Analysis Date = 04/24/16 Pct Recovery = 100% Analysis Date = 04/19/16 Pct Recovery = 100% Analysis Date = 04/19/16 Pct Recovery = 100% Analysis Date = 04/15/16 Pct Recovery = 100% Analysis Date = 04/15/16 Pct Recovery = 100% Analysis Date = 04/10/16 Pct Recovery = 100% Analysis Date = 04/10/16 Pct Recovery = 100% Analysis Date = 04/05/16 Pct Recovery = 100% Analysis Date = 04/05/16 Pct Recovery = 100% Analysis Date = 03/31/16 Pct Recovery = 100% Analysis Date = 03/31/16 Pct Recovery = 100% Analysis Date = 03/26/16 Pct Recovery = 100% Analysis Date = 03/26/16 Pct Recovery = 100% Analysis Date = 03/22/16 Pct Recovery = 100% Analysis Date = 03/22/16 Pct Recovery = 100% Analysis Date = 03/17/16 Pct Recovery = 100% Analysis Date = 03/17/16 Pct Recovery = 100% Analysis Date = 03/12/16 Pct Recovery = 100% Analysis Date = 03/12/16 Pct Recovery = 100% Analysis Date = 03/07/16 Pct Recovery = 100% Analysis Date = 03/07/16 Pct Recovery = 100% Analysis Date = 03/02/16 Pct Recovery = 100% Analysis Date = 03/02/16 Pct Recovery = 100% Analysis Date = 02/27/16 Pct Recovery = 99% Analysis Date = 02/27/16 Pct Recovery = 99% Analysis Date = 02/22/16 Pct Recovery = 99% Analysis Date = 02/22/16 Pct Recovery = 99% Analysis Date = 02/17/16 Pct Recovery = 99% Analysis Date = 02/17/16 Pct Recovery = 99% Analysis Date = 02/12/16 Pct Recovery = 99% Analysis Date = 02/12/16 Pct Recovery = 99% Analysis Date = 02/07/16 Pct Recovery = 99% Analysis Date = 02/07/16 Pct Recovery = 99% Analysis Date = 02/03/16 Pct Recovery = 99% Analysis Date = 02/03/16 Pct Recovery = 99% Analysis Date = 01/29/16 Pct Recovery = 99% Analysis Date = 01/29/16 Pct Recovery = 99% Analysis Date = 01/24/16 Pct Recovery = 99% Analysis Date = 01/24/16 Pct Recovery = 99% Analysis Date = 01/19/16 Pct Recovery = 99% Analysis Date = 01/19/16 Pct Recovery = 99% Analysis Date = 01/14/16 Pct Recovery = 99% Analysis Date = 01/14/16 Pct Recovery = 99% Analysis Date = 01/10/16 Pct Recovery = 99% Analysis Date = 01/10/16 Pct Recovery = 99% Analysis Date = 01/05/16 Pct Recovery = 99% Analysis Date = 01/05/16 Pct Recovery = 99% Analysis Date = 12/31/15 Pct Recovery = 99% Analysis Date = 12/31/15 Pct Recovery = 99% Analysis Date = 12/26/15 Pct Recovery = 99% Analysis Date = 12/26/15 Pct Recovery = 99% Analysis Date = 12/21/15 Pct Recovery = 99% Analysis Date = 12/21/15 Pct Recovery = 99% Analysis Date = 12/17/15 Pct Recovery = 99% Analysis Date = 12/17/15 Pct Recovery = 99% Analysis Date = 12/12/15 Pct Recovery = 99% Analysis Date = 12/12/15 Pct Recovery = 99% Analysis Date = 12/07/15 Pct Recovery = 99% Analysis Date = 12/07/15 Pct Recovery = 99% Analysis Date = 12/02/15 Pct Recovery = 99% Analysis Date = 12/02/15 Pct Recovery = 99% Analysis Date = 11/27/15 Pct Recovery = 99% Analysis Date = 11/27/15 Pct Recovery = 99% Analysis Date = 11/23/15 Pct Recovery = 99% Analysis Date = 11/23/15 Pct Recovery = 99% Analysis Date = 11/18/15 Pct Recovery = 99% Analysis Date = 11/18/15 Pct Recovery = 99% Analysis Date = 11/13/15 Pct Recovery = 99% Analysis Date = 11/13/15 Pct Recovery = 99% Analysis Date = 11/08/15 Pct Recovery = 99% Analysis Date = 11/08/15 Pct Recovery = 99% Analysis Date = 11/03/15 Pct Recovery = 99% Analysis Date = 11/03/15 Pct Recovery = 99% Analysis Date = 10/30/15 Pct Recovery = 99% Analysis Date = 10/30/15 Pct Recovery = 99% Analysis Date = 10/25/15 Pct Recovery = 99% Analysis Date = 10/25/15 Pct Recovery = 99% Analysis Date = 10/20/15 Pct Recovery = 99% Analysis Date = 10/20/15 Pct Recovery = 99% Analysis Date = 10/15/15 Pct Recovery = 99% Analysis Date = 10/15/15 Pct Recovery = 99% Analysis Date = 10/10/15 Pct Recovery = 99% Analysis Date = 10/10/15 Pct Recovery = 99% Analysis Date = 10/06/15 Pct Recovery = 99% Analysis Date = 10/06/15 Pct Recovery = 99% Analysis Date = 10/01/15 Pct Recovery = 99% Analysis Date = 10/01/15 Pct Recovery = 99% Analysis Date = 09/26/15 Pct Recovery = 99% Analysis Date = 09/26/15 Pct Recovery = 99% Analysis Date = 09/21/15 Pct Recovery = 99% Analysis Date = 09/21/15 Pct Recovery = 99% Analysis Date = 09/16/15 Pct Recovery = 99% Analysis Date = 09/16/15 Pct Recovery = 99% Analysis Date = 09/12/15 Pct Recovery = 99% Analysis Date = 09/12/15 Pct Recovery = 99% Analysis Date = 09/07/15 Pct Recovery = 99% Analysis Date = 09/07/15 Pct Recovery = 99% Analysis Date = 09/02/15 Pct Recovery = 99% Analysis Date = 09/02/15 Pct Recovery = 99% Analysis Date = 08/28/15 Pct Recovery = 99% Analysis Date = 08/28/15 Pct Recovery = 99% Analysis Date = 08/23/15 Pct Recovery = 99% Analysis Date = 08/23/15 Pct Recovery = 99% Analysis Date = 08/19/15 Pct Recovery = 99% Analysis Date = 08/19/15 Pct Recovery = 99% Analysis Date = 08/14/15 Pct Recovery = 99% Analysis Date = 08/14/15 Pct Recovery = 99% Analysis Date = 08/09/15 Pct Recovery = 99% Analysis Date = 08/09/15 Pct Recovery = 99% Analysis Date = 08/04/15 Pct Recovery = 99% Analysis Date = 08/04/15 Pct Recovery = 99% Analysis Date = 07/30/15 Pct Recovery = 99% Analysis Date = 07/30/15 Pct Recovery = 99% Analysis Date = 07/26/15 Pct Recovery = 99% Analysis Date = 07/26/15 Pct Recovery = 99% Analysis Date = 07/21/15 Pct Recovery = 99% Analysis Date = 07/21/15 Pct Recovery = 99% Analysis Date = 07/16/15 Pct Recovery = 99% Analysis Date = 07/16/15 Pct Recovery = 99% Analysis Date = 07/11/15 Pct Recovery = 99% Analysis Date = 07/11/15 Pct Recovery = 99% Analysis Date = 07/06/15 Pct Recovery = 99% Analysis Date = 07/06/15 Pct Recovery = 99% Analysis Date = 07/02/15 Pct Recovery = 99% Analysis Date = 07/02/15 Pct Recovery = 99% Analysis Date = 06/27/15 Pct Recovery = 99% Analysis Date = 06/27/15 Pct Recovery = 99% Analysis Date = 06/22/15 Pct Recovery = 99% Analysis Date = 06/22/15 Pct Recovery = 99% Analysis Date = 06/17/15 Pct Recovery = 99% Analysis Date = 06/17/15 Pct Recovery = 99% Analysis Date = 06/12/15 Pct Recovery = 99% Analysis Date = 06/12/15 Pct Recovery = 99% Analysis Date = 06/08/15 Pct Recovery = 100% Analysis Date = 06/08/15 Pct Recovery = 100% Analysis Date = 06/03/15 Pct Recovery = 100% Analysis Date = 06/03/15 Pct Recovery = 100% Analysis Date = 05/29/15 Pct Recovery = 100% Analysis Date = 05/29/15 Pct Recovery = 100% Analysis Date = 05/24/15 Pct Recovery = 100% Analysis Date = 05/24/15 Pct Recovery = 100% Analysis Date = 05/19/15 Pct Recovery = 100% Analysis Date = 05/19/15 Pct Recovery = 100% Analysis Date = 05/15/15 Pct Recovery = 100% Analysis Date = 05/15/15 Pct Recovery = 100% Analysis Date = 05/10/15 Pct Recovery = 100% Analysis Date = 05/10/15 Pct Recovery = 100% Analysis Date = 05/05/15 Pct Recovery = 100% Analysis Date = 05/05/15 Pct Recovery = 100% Analysis Date = 04/30/15 Pct Recovery = 100% Analysis Date = 04/30/15 Pct Recovery = 100% Analysis Date = 04/25/15 Pct Recovery = 100% Analysis Date = 04/25/15 Pct Recovery = 100% Analysis Date = 04/21/15 Pct Recovery = 100% Analysis Date = 04/21/15 Pct Recovery = 100% Analysis Date = 04/16/15 Pct Recovery = 100% Analysis Date = 04/16/15 Pct Recovery = 100% Analysis Date = 04/11/15 Pct Recovery = 100% Analysis Date = 04/11/15 Pct Recovery = 100% Analysis Date = 04/06/15 Pct Recovery = 100% Analysis Date = 04/06/15 Pct Recovery = 100% Analysis Date = 04/01/15 Pct Recovery = 100% Analysis Date = 04/01/15 Pct Recovery = 100% Analysis Date = 03/28/15 Pct Recovery = 100% Analysis Date = 03/28/15 Pct Recovery = 100% Analysis Date = 03/23/15 Pct Recovery = 100% Analysis Date = 03/23/15 Pct Recovery = 100% Analysis Date = 03/18/15 Pct Recovery = 100% Analysis Date = 03/18/15 Pct Recovery = 100% Analysis Date = 03/13/15 Pct Recovery = 100% Analysis Date = 03/13/15 Pct Recovery = 100% Analysis Date = 03/08/15 Pct Recovery = 100% Analysis Date = 03/08/15 Pct Recovery = 100% Analysis Date = 03/04/15 Pct Recovery = 100% Analysis Date = 03/04/15 Pct Recovery = 100% Analysis Date = 02/27/15 Pct Recovery = 100% Analysis Date = 02/27/15 Pct Recovery = 100% Analysis Date = 02/22/15 Pct Recovery = 100% Analysis Date = 02/22/15 Pct Recovery = 100% Analysis Date = 02/17/15 Pct Recovery = 100% Analysis Date = 02/17/15 Pct Recovery = 100% Analysis Date = 02/12/15 Pct Recovery = 101% Analysis Date = 02/12/15 Pct Recovery = 101% Analysis Date = 02/08/15 Pct Recovery = 101% Analysis Date = 02/08/15 Pct Recovery = 101% Analysis Date = 02/03/15 Pct Recovery = 101% Analysis Date = 02/03/15 Pct Recovery = 101% Analysis Date = 01/29/15 Pct Recovery = 101% Analysis Date = 01/29/15 Pct Recovery = 101% Analysis Date = 01/24/15 Pct Recovery = 101% Analysis Date = 01/24/15 Pct Recovery = 101% Analysis Date = 01/19/15 Pct Recovery = 101% Analysis Date = 01/19/15 Pct Recovery = 101% Analysis Date = 01/15/15 Pct Recovery = 101% Analysis Date = 01/15/15 Pct Recovery = 101% Analysis Date = 01/10/15 Pct Recovery = 101% Analysis Date = 01/10/15 Pct Recovery = 101% Analysis Date = 01/05/15 Pct Recovery = 101% Analysis Date = 01/05/15 Pct Recovery = 101% Analysis Date = 12/31/14 Pct Recovery = 101% Analysis Date = 12/31/14 Pct Recovery = 101% Analysis Date = 12/26/14 Pct Recovery = 101% Analysis Date = 12/26/14 Pct Recovery = 101% Analysis Date = 12/22/14 Pct Recovery = 101% Analysis Date = 12/22/14 Pct Recovery = 101% Analysis Date = 12/17/14 Pct Recovery = 101% Analysis Date = 12/17/14 Pct Recovery = 101% Analysis Date = 12/12/14 Pct Recovery = 101% Analysis Date = 12/12/14 Pct Recovery = 101% Analysis Date = 12/07/14 Pct Recovery = 101% Analysis Date = 12/07/14 Pct Recovery = 101% Analysis Date = 12/02/14 Pct Recovery = 101% Analysis Date = 12/02/14 Pct Recovery = 101% Analysis Date = 11/28/14 Pct Recovery = 101% Analysis Date = 11/28/14 Pct Recovery = 101% Analysis Date = 11/23/14 Pct Recovery = 102% Analysis Date = 11/23/14 Pct Recovery = 102% Analysis Date = 11/18/14 Pct Recovery = 102% Analysis Date = 11/18/14 Pct Recovery = 102% Analysis Date = 11/13/14 Pct Recovery = 102% Analysis Date = 11/13/14 Pct Recovery = 102% Analysis Date = 11/08/14 Pct Recovery = 102% Analysis Date = 11/08/14 Pct Recovery = 102% Analysis Date = 11/04/14 Pct Recovery = 102% Analysis Date = 11/04/14 Pct Recovery = 102% Analysis Date = 10/30/14 Pct Recovery = 102% Analysis Date = 10/30/14 Pct Recovery = 102% Analysis Date = 10/25/14 Pct Recovery = 102% Analysis Date = 10/25/14 Pct Recovery = 102% Analysis Date = 10/20/14 Pct Recovery = 102% Analysis Date = 10/20/14 Pct Recovery = 102% Analysis Date = 10/15/14 Pct Recovery = 102% Analysis Date = 10/15/14 Pct Recovery = 102% Analysis Date = 10/11/14 Pct Recovery = 102% Analysis Date = 10/11/14 Pct Recovery = 102% Analysis Date = 10/06/14 Pct Recovery = 102% Analysis Date = 10/06/14 Pct Recovery = 102% Analysis Date = 10/01/14 Pct Recovery = 102% Analysis Date = 10/01/14 Pct Recovery = 102% Analysis Date = 09/26/14 Pct Recovery = 102% Analysis Date = 09/26/14 Pct Recovery = 102% Analysis Date = 09/21/14 Pct Recovery = 102% Analysis Date = 09/21/14 Pct Recovery = 102% Analysis Date = 09/17/14 Pct Recovery = 102% Analysis Date = 09/17/14 Pct Recovery = 102% Analysis Date = 09/12/14 Pct Recovery = 102% Analysis Date = 09/12/14 Pct Recovery = 102% Analysis Date = 09/07/14 Pct Recovery = 102% Analysis Date = 09/07/14 Pct Recovery = 102% Analysis Date = 09/02/14 Pct Recovery = 102% Analysis Date = 09/02/14 Pct Recovery = 102% Analysis Date = 08/28/14 Pct Recovery = 102% Analysis Date = 08/28/14 Pct Recovery = 102% Analysis Date = 08/24/14 Pct Recovery = 102% Analysis Date = 08/24/14 Pct Recovery = 102% Analysis Date = 08/19/14 Pct Recovery = 103% Analysis Date = 08/19/14 Pct Recovery = 103% Analysis Date = 08/14/14 Pct Recovery = 103% Analysis Date = 08/14/14 Pct Recovery = 103% Analysis Date = 08/09/14 Pct Recovery = 103% Analysis Date = 08/09/14 Pct Recovery = 103% Analysis Date = 08/04/14 Pct Recovery = 103% Analysis Date = 08/04/14 Pct Recovery = 103% Analysis Date = 07/31/14 Pct Recovery = 103% Analysis Date = 07/31/14 Pct Recovery = 103% Analysis Date = 07/26/14 Pct Recovery = 103% Analysis Date = 07/26/14 Pct Recovery = 103% Analysis Date = 07/21/14 Pct Recovery = 103% Analysis Date = 07/21/14 Pct Recovery = 103% Analysis Date = 07/16/14 Pct Recovery = 103% Analysis Date = 07/16/14 Pct Recovery = 103% Analysis Date = 07/11/14 Pct Recovery = 103% Analysis Date = 07/11/14 Pct Recovery = 103% Analysis Date = 07/07/14 Pct Recovery = 103% Analysis Date = 07/07/14 Pct Recovery = 103% Analysis Date = 07/02/14 Pct Recovery = 103% Analysis Date = 07/02/14 Pct Recovery = 103% Analysis Date = 06/27/14 Pct Recovery = 103% Analysis Date = 06/27/14 Pct Recovery = 103% Analysis Date = 06/22/14 Pct Recovery = 103% Analysis Date = 06/22/14 Pct Recovery = 103% Analysis Date = 06/17/14 Pct Recovery = 103% Analysis Date = 06/17/14 Pct Recovery = 103% Analysis Date = 06/13/14 Pct Recovery = 103% Analysis Date = 06/13/14 Pct Recovery = 103% Analysis Date = 06/08/14 Pct Recovery = 103% Analysis Date = 06/08/14 Pct Recovery = 103% Analysis Date = 06/03/14 Pct Recovery = 103% Analysis Date = 06/03/14 Pct Recovery = 103% Analysis Date = 05/29/14 Pct Recovery = 103% Analysis Date = 05/29/14 Pct Recovery = 103% Analysis Date = 05/24/14 Pct Recovery = 103% Analysis Date = 05/24/14 Pct Recovery = 103% Analysis Date = 05/20/14 Pct Recovery = 103% Analysis Date = 05/20/14 Pct Recovery = 103% Analysis Date = 05/15/14 Pct Recovery = 103% Analysis Date = 05/15/14 Pct Recovery = 103% Analysis Date = 05/10/14 Pct Recovery = 104% Analysis Date = 05/10/14 Pct Recovery = 104% Analysis Date = 05/05/14 Pct Recovery = 104% Analysis Date = 05/05/14 Pct Recovery = 104% Analysis Date = 05/01/14 Pct Recovery = 104% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
METHYL ACRYLONITRILE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 49 101% 7% 100% 8%
Total 49 101% 7% 100% 8%

Sample Statistics
METHYL ACRYLONITRILE

Characteristic N % % Basis
Plotted 49 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 49 .  
False Negatives 0 0% 0 out of 49
Not Spiked 24 .  
False Positives 0 0% 0 out of 24

BQS OBSP Determination:
METHYL IODIDE
METHOD: 4440 , TESTIDCODE: 77424GCM66
Open Data Set

Analysis Date = 12/16/16 SpikeMix = NSI 041816AVOC: 40 µl & ChemService 5082900: 40 µl Pct Recovery = 113% Analysis Date = 08/04/16 SpikeMix = Crescent 03FF058: 40 µl & Supelco LC20141V: 40 µl Pct Recovery = 62% Analysis Date = 07/20/16 SpikeMix = Supelco LC20141V: 40 µl & Accu 216041125: 40 µl Pct Recovery = 91% Analysis Date = 11/21/16 SpikeMix = Crescent 03FF058: 25 µl & Supelco LC20141V: 25 µl Pct Recovery = 84% Analysis Date = 09/08/16 SpikeMix = Supelco LC20141V: 25 µl & Accu 216041125: 25 µl Pct Recovery = 63% Analysis Date = 08/26/16 SpikeMix = NSI 041816AVOC: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 113% Analysis Date = 08/12/16 SpikeMix = ChemService 5082900: 25 µl & Phenova B20160319: 25 µl Pct Recovery = 93% Analysis Date = 07/06/16 SpikeMix = Crescent 03FF058: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 76% Analysis Date = 08/15/15 SpikeMix = Supelco LC13545: 25 µl & Crescent 04EE008: 25 µl Pct Recovery = 108% Analysis Date = 06/16/15 SpikeMix = ERA 0406-15-03: 25 µl & Supelco LC13545: 25 µl Pct Recovery = 109% Analysis Date = 02/28/15 SpikeMix = ERA 0227-14-06.1A: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 75% Analysis Date = 12/17/14 SpikeMix = Supelco LC06438: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 57% Analysis Date = 09/21/14 SpikeMix = Supelco LC06438: 20 µl Pct Recovery = 67% Analysis Date = 06/10/14 SpikeMix = NSI 032614: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 127% Analysis Date = 03/19/15 SpikeMix = Spex Organics C1140417015: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 91% Analysis Date = 11/22/14 SpikeMix = NSI 032614: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 77% Analysis Date = 08/19/14 SpikeMix = Spex Organics C1140417015: 20 µl & Accu 214031115: 20 µl Pct Recovery = 79% Analysis Date = 08/16/14 SpikeMix = ERA 0227-14-06.1A: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 80% Analysis Date = 11/29/16 SpikeMix = ChemService 5082900: 15 µl & Phenova B20160319: 15 µl Pct Recovery = 114% Analysis Date = 10/13/16 SpikeMix = NSI 041816AVOC: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 101% Analysis Date = 09/28/16 SpikeMix = Crescent 03FF058: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 114% Analysis Date = 07/06/16 SpikeMix = ChemService 5082900: 15 µl & Accu 216041125: 15 µl Pct Recovery = 116% Analysis Date = 06/15/16 SpikeMix = NSI 041816AVOC: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 63% Analysis Date = 05/27/16 SpikeMix = Phenova B20160319: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 93% Analysis Date = 04/26/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 178% Analysis Date = 02/05/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 89% Analysis Date = 11/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 90% Analysis Date = 10/16/15 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 105% Analysis Date = 06/29/15 SpikeMix = Spex Organics EN150428007: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 116% Analysis Date = 04/02/16 SpikeMix = Supelco LC13545: 15 µl & Accu 215041380: 15 µl Pct Recovery = 88% Analysis Date = 12/18/15 SpikeMix = Supelco LC13545: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 103% Analysis Date = 10/21/14 SpikeMix = ERA 0227-14-06.1A: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 67% Analysis Date = 06/18/14 SpikeMix = Supelco LC06438: 10 µl & Accu 214031115: 10 µl Pct Recovery = 90% Analysis Date = 05/30/14 SpikeMix = NSI 032614: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 116% Analysis Date = 05/03/14 SpikeMix = Crescent 03DD004: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 34% Analysis Date = 02/18/16 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 113% Analysis Date = 11/20/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 101% Analysis Date = 09/03/15 SpikeMix = NSI 050515AVOC: 10 µl & Spex Organics EN150428007: 10 µl Pct Recovery = 107% Analysis Date = 06/04/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 130% Analysis Date = 11/06/14 SpikeMix = Spex Organics C1140417015: 10 µl & Crescent 03DD004: 10 µl Pct Recovery = 39% Analysis Date = 09/09/14 SpikeMix = NSI 032614: 10 µl & Spex Organics C1140417015: 10 µl Pct Recovery = 138% Analysis Date = 07/23/14 SpikeMix = Spex Organics C1140417015: 10 µl & Accu 214031115: 10 µl Pct Recovery = 101% Analysis Date = 07/11/14 SpikeMix = Spex Organics C1140417015: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 71% Analysis Date = 05/13/16 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 106% Analysis Date = 03/17/16 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 81% Analysis Date = 12/10/15 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 98% Analysis Date = 06/29/15 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 108% Analysis Date = 06/27/15 SpikeMix = ERA 0406-15-03: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 96% Analysis Date = 12/16/16 Pct Recovery = 96% Analysis Date = 12/11/16 Pct Recovery = 96% Analysis Date = 12/11/16 Pct Recovery = 96% Analysis Date = 12/06/16 Pct Recovery = 96% Analysis Date = 12/06/16 Pct Recovery = 96% Analysis Date = 12/01/16 Pct Recovery = 96% Analysis Date = 12/01/16 Pct Recovery = 96% Analysis Date = 11/26/16 Pct Recovery = 97% Analysis Date = 11/26/16 Pct Recovery = 97% Analysis Date = 11/22/16 Pct Recovery = 97% Analysis Date = 11/22/16 Pct Recovery = 97% Analysis Date = 11/17/16 Pct Recovery = 97% Analysis Date = 11/17/16 Pct Recovery = 97% Analysis Date = 11/12/16 Pct Recovery = 97% Analysis Date = 11/12/16 Pct Recovery = 97% Analysis Date = 11/07/16 Pct Recovery = 97% Analysis Date = 11/07/16 Pct Recovery = 97% Analysis Date = 11/02/16 Pct Recovery = 97% Analysis Date = 11/02/16 Pct Recovery = 97% Analysis Date = 10/29/16 Pct Recovery = 97% Analysis Date = 10/29/16 Pct Recovery = 97% Analysis Date = 10/24/16 Pct Recovery = 97% Analysis Date = 10/24/16 Pct Recovery = 97% Analysis Date = 10/19/16 Pct Recovery = 97% Analysis Date = 10/19/16 Pct Recovery = 97% Analysis Date = 10/14/16 Pct Recovery = 97% Analysis Date = 10/14/16 Pct Recovery = 97% Analysis Date = 10/09/16 Pct Recovery = 97% Analysis Date = 10/09/16 Pct Recovery = 97% Analysis Date = 10/05/16 Pct Recovery = 97% Analysis Date = 10/05/16 Pct Recovery = 97% Analysis Date = 09/30/16 Pct Recovery = 97% Analysis Date = 09/30/16 Pct Recovery = 97% Analysis Date = 09/25/16 Pct Recovery = 97% Analysis Date = 09/25/16 Pct Recovery = 97% Analysis Date = 09/20/16 Pct Recovery = 97% Analysis Date = 09/20/16 Pct Recovery = 97% Analysis Date = 09/15/16 Pct Recovery = 97% Analysis Date = 09/15/16 Pct Recovery = 97% Analysis Date = 09/11/16 Pct Recovery = 97% Analysis Date = 09/11/16 Pct Recovery = 97% Analysis Date = 09/06/16 Pct Recovery = 97% Analysis Date = 09/06/16 Pct Recovery = 97% Analysis Date = 09/01/16 Pct Recovery = 97% Analysis Date = 09/01/16 Pct Recovery = 97% Analysis Date = 08/27/16 Pct Recovery = 97% Analysis Date = 08/27/16 Pct Recovery = 97% Analysis Date = 08/23/16 Pct Recovery = 97% Analysis Date = 08/23/16 Pct Recovery = 97% Analysis Date = 08/18/16 Pct Recovery = 97% Analysis Date = 08/18/16 Pct Recovery = 97% Analysis Date = 08/13/16 Pct Recovery = 97% Analysis Date = 08/13/16 Pct Recovery = 97% Analysis Date = 08/08/16 Pct Recovery = 97% Analysis Date = 08/08/16 Pct Recovery = 97% Analysis Date = 08/03/16 Pct Recovery = 97% Analysis Date = 08/03/16 Pct Recovery = 97% Analysis Date = 07/30/16 Pct Recovery = 97% Analysis Date = 07/30/16 Pct Recovery = 97% Analysis Date = 07/25/16 Pct Recovery = 97% Analysis Date = 07/25/16 Pct Recovery = 97% Analysis Date = 07/20/16 Pct Recovery = 97% Analysis Date = 07/20/16 Pct Recovery = 97% Analysis Date = 07/15/16 Pct Recovery = 97% Analysis Date = 07/15/16 Pct Recovery = 97% Analysis Date = 07/10/16 Pct Recovery = 97% Analysis Date = 07/10/16 Pct Recovery = 97% Analysis Date = 07/06/16 Pct Recovery = 97% Analysis Date = 07/06/16 Pct Recovery = 97% Analysis Date = 07/01/16 Pct Recovery = 97% Analysis Date = 07/01/16 Pct Recovery = 97% Analysis Date = 06/26/16 Pct Recovery = 97% Analysis Date = 06/26/16 Pct Recovery = 97% Analysis Date = 06/21/16 Pct Recovery = 97% Analysis Date = 06/21/16 Pct Recovery = 97% Analysis Date = 06/16/16 Pct Recovery = 97% Analysis Date = 06/16/16 Pct Recovery = 97% Analysis Date = 06/12/16 Pct Recovery = 97% Analysis Date = 06/12/16 Pct Recovery = 97% Analysis Date = 06/07/16 Pct Recovery = 97% Analysis Date = 06/07/16 Pct Recovery = 97% Analysis Date = 06/02/16 Pct Recovery = 98% Analysis Date = 06/02/16 Pct Recovery = 98% Analysis Date = 05/28/16 Pct Recovery = 98% Analysis Date = 05/28/16 Pct Recovery = 98% Analysis Date = 05/24/16 Pct Recovery = 98% Analysis Date = 05/24/16 Pct Recovery = 98% Analysis Date = 05/19/16 Pct Recovery = 98% Analysis Date = 05/19/16 Pct Recovery = 98% Analysis Date = 05/14/16 Pct Recovery = 98% Analysis Date = 05/14/16 Pct Recovery = 98% Analysis Date = 05/09/16 Pct Recovery = 98% Analysis Date = 05/09/16 Pct Recovery = 98% Analysis Date = 05/04/16 Pct Recovery = 98% Analysis Date = 05/04/16 Pct Recovery = 98% Analysis Date = 04/30/16 Pct Recovery = 98% Analysis Date = 04/30/16 Pct Recovery = 98% Analysis Date = 04/25/16 Pct Recovery = 98% Analysis Date = 04/25/16 Pct Recovery = 98% Analysis Date = 04/20/16 Pct Recovery = 98% Analysis Date = 04/20/16 Pct Recovery = 98% Analysis Date = 04/15/16 Pct Recovery = 98% Analysis Date = 04/15/16 Pct Recovery = 98% Analysis Date = 04/10/16 Pct Recovery = 98% Analysis Date = 04/10/16 Pct Recovery = 98% Analysis Date = 04/06/16 Pct Recovery = 99% Analysis Date = 04/06/16 Pct Recovery = 99% Analysis Date = 04/01/16 Pct Recovery = 99% Analysis Date = 04/01/16 Pct Recovery = 99% Analysis Date = 03/27/16 Pct Recovery = 99% Analysis Date = 03/27/16 Pct Recovery = 99% Analysis Date = 03/22/16 Pct Recovery = 99% Analysis Date = 03/22/16 Pct Recovery = 99% Analysis Date = 03/17/16 Pct Recovery = 99% Analysis Date = 03/17/16 Pct Recovery = 99% Analysis Date = 03/13/16 Pct Recovery = 99% Analysis Date = 03/13/16 Pct Recovery = 99% Analysis Date = 03/08/16 Pct Recovery = 100% Analysis Date = 03/08/16 Pct Recovery = 100% Analysis Date = 03/03/16 Pct Recovery = 100% Analysis Date = 03/03/16 Pct Recovery = 100% Analysis Date = 02/27/16 Pct Recovery = 100% Analysis Date = 02/27/16 Pct Recovery = 100% Analysis Date = 02/23/16 Pct Recovery = 100% Analysis Date = 02/23/16 Pct Recovery = 100% Analysis Date = 02/18/16 Pct Recovery = 100% Analysis Date = 02/18/16 Pct Recovery = 100% Analysis Date = 02/13/16 Pct Recovery = 100% Analysis Date = 02/13/16 Pct Recovery = 100% Analysis Date = 02/08/16 Pct Recovery = 101% Analysis Date = 02/08/16 Pct Recovery = 101% Analysis Date = 02/03/16 Pct Recovery = 101% Analysis Date = 02/03/16 Pct Recovery = 101% Analysis Date = 01/30/16 Pct Recovery = 101% Analysis Date = 01/30/16 Pct Recovery = 101% Analysis Date = 01/25/16 Pct Recovery = 101% Analysis Date = 01/25/16 Pct Recovery = 101% Analysis Date = 01/20/16 Pct Recovery = 101% Analysis Date = 01/20/16 Pct Recovery = 101% Analysis Date = 01/15/16 Pct Recovery = 102% Analysis Date = 01/15/16 Pct Recovery = 102% Analysis Date = 01/10/16 Pct Recovery = 102% Analysis Date = 01/10/16 Pct Recovery = 102% Analysis Date = 01/06/16 Pct Recovery = 102% Analysis Date = 01/06/16 Pct Recovery = 102% Analysis Date = 01/01/16 Pct Recovery = 102% Analysis Date = 01/01/16 Pct Recovery = 102% Analysis Date = 12/27/15 Pct Recovery = 102% Analysis Date = 12/27/15 Pct Recovery = 102% Analysis Date = 12/22/15 Pct Recovery = 103% Analysis Date = 12/22/15 Pct Recovery = 103% Analysis Date = 12/17/15 Pct Recovery = 103% Analysis Date = 12/17/15 Pct Recovery = 103% Analysis Date = 12/13/15 Pct Recovery = 103% Analysis Date = 12/13/15 Pct Recovery = 103% Analysis Date = 12/08/15 Pct Recovery = 103% Analysis Date = 12/08/15 Pct Recovery = 103% Analysis Date = 12/03/15 Pct Recovery = 103% Analysis Date = 12/03/15 Pct Recovery = 103% Analysis Date = 11/28/15 Pct Recovery = 103% Analysis Date = 11/28/15 Pct Recovery = 103% Analysis Date = 11/24/15 Pct Recovery = 103% Analysis Date = 11/24/15 Pct Recovery = 103% Analysis Date = 11/19/15 Pct Recovery = 103% Analysis Date = 11/19/15 Pct Recovery = 103% Analysis Date = 11/14/15 Pct Recovery = 104% Analysis Date = 11/14/15 Pct Recovery = 104% Analysis Date = 11/09/15 Pct Recovery = 104% Analysis Date = 11/09/15 Pct Recovery = 104% Analysis Date = 11/04/15 Pct Recovery = 104% Analysis Date = 11/04/15 Pct Recovery = 104% Analysis Date = 10/31/15 Pct Recovery = 104% Analysis Date = 10/31/15 Pct Recovery = 104% Analysis Date = 10/26/15 Pct Recovery = 104% Analysis Date = 10/26/15 Pct Recovery = 104% Analysis Date = 10/21/15 Pct Recovery = 104% Analysis Date = 10/21/15 Pct Recovery = 104% Analysis Date = 10/16/15 Pct Recovery = 104% Analysis Date = 10/16/15 Pct Recovery = 104% Analysis Date = 10/11/15 Pct Recovery = 104% Analysis Date = 10/11/15 Pct Recovery = 104% Analysis Date = 10/07/15 Pct Recovery = 104% Analysis Date = 10/07/15 Pct Recovery = 104% Analysis Date = 10/02/15 Pct Recovery = 103% Analysis Date = 10/02/15 Pct Recovery = 103% Analysis Date = 09/27/15 Pct Recovery = 103% Analysis Date = 09/27/15 Pct Recovery = 103% Analysis Date = 09/22/15 Pct Recovery = 103% Analysis Date = 09/22/15 Pct Recovery = 103% Analysis Date = 09/17/15 Pct Recovery = 103% Analysis Date = 09/17/15 Pct Recovery = 103% Analysis Date = 09/13/15 Pct Recovery = 102% Analysis Date = 09/13/15 Pct Recovery = 102% Analysis Date = 09/08/15 Pct Recovery = 102% Analysis Date = 09/08/15 Pct Recovery = 102% Analysis Date = 09/03/15 Pct Recovery = 102% Analysis Date = 09/03/15 Pct Recovery = 102% Analysis Date = 08/29/15 Pct Recovery = 102% Analysis Date = 08/29/15 Pct Recovery = 102% Analysis Date = 08/25/15 Pct Recovery = 101% Analysis Date = 08/25/15 Pct Recovery = 101% Analysis Date = 08/20/15 Pct Recovery = 101% Analysis Date = 08/20/15 Pct Recovery = 101% Analysis Date = 08/15/15 Pct Recovery = 101% Analysis Date = 08/15/15 Pct Recovery = 101% Analysis Date = 08/10/15 Pct Recovery = 101% Analysis Date = 08/10/15 Pct Recovery = 101% Analysis Date = 08/05/15 Pct Recovery = 100% Analysis Date = 08/05/15 Pct Recovery = 100% Analysis Date = 08/01/15 Pct Recovery = 100% Analysis Date = 08/01/15 Pct Recovery = 100% Analysis Date = 07/27/15 Pct Recovery = 100% Analysis Date = 07/27/15 Pct Recovery = 100% Analysis Date = 07/22/15 Pct Recovery = 100% Analysis Date = 07/22/15 Pct Recovery = 100% Analysis Date = 07/17/15 Pct Recovery = 99% Analysis Date = 07/17/15 Pct Recovery = 99% Analysis Date = 07/12/15 Pct Recovery = 99% Analysis Date = 07/12/15 Pct Recovery = 99% Analysis Date = 07/08/15 Pct Recovery = 99% Analysis Date = 07/08/15 Pct Recovery = 99% Analysis Date = 07/03/15 Pct Recovery = 99% Analysis Date = 07/03/15 Pct Recovery = 99% Analysis Date = 06/28/15 Pct Recovery = 98% Analysis Date = 06/28/15 Pct Recovery = 98% Analysis Date = 06/23/15 Pct Recovery = 98% Analysis Date = 06/23/15 Pct Recovery = 98% Analysis Date = 06/18/15 Pct Recovery = 97% Analysis Date = 06/18/15 Pct Recovery = 97% Analysis Date = 06/14/15 Pct Recovery = 97% Analysis Date = 06/14/15 Pct Recovery = 97% Analysis Date = 06/09/15 Pct Recovery = 96% Analysis Date = 06/09/15 Pct Recovery = 96% Analysis Date = 06/04/15 Pct Recovery = 96% Analysis Date = 06/04/15 Pct Recovery = 96% Analysis Date = 05/30/15 Pct Recovery = 96% Analysis Date = 05/30/15 Pct Recovery = 96% Analysis Date = 05/25/15 Pct Recovery = 96% Analysis Date = 05/25/15 Pct Recovery = 96% Analysis Date = 05/21/15 Pct Recovery = 95% Analysis Date = 05/21/15 Pct Recovery = 95% Analysis Date = 05/16/15 Pct Recovery = 95% Analysis Date = 05/16/15 Pct Recovery = 95% Analysis Date = 05/11/15 Pct Recovery = 95% Analysis Date = 05/11/15 Pct Recovery = 95% Analysis Date = 05/06/15 Pct Recovery = 95% Analysis Date = 05/06/15 Pct Recovery = 95% Analysis Date = 05/02/15 Pct Recovery = 94% Analysis Date = 05/02/15 Pct Recovery = 94% Analysis Date = 04/27/15 Pct Recovery = 94% Analysis Date = 04/27/15 Pct Recovery = 94% Analysis Date = 04/22/15 Pct Recovery = 94% Analysis Date = 04/22/15 Pct Recovery = 94% Analysis Date = 04/17/15 Pct Recovery = 93% Analysis Date = 04/17/15 Pct Recovery = 93% Analysis Date = 04/12/15 Pct Recovery = 93% Analysis Date = 04/12/15 Pct Recovery = 93% Analysis Date = 04/08/15 Pct Recovery = 93% Analysis Date = 04/08/15 Pct Recovery = 93% Analysis Date = 04/03/15 Pct Recovery = 93% Analysis Date = 04/03/15 Pct Recovery = 93% Analysis Date = 03/29/15 Pct Recovery = 92% Analysis Date = 03/29/15 Pct Recovery = 92% Analysis Date = 03/24/15 Pct Recovery = 92% Analysis Date = 03/24/15 Pct Recovery = 92% Analysis Date = 03/19/15 Pct Recovery = 92% Analysis Date = 03/19/15 Pct Recovery = 92% Analysis Date = 03/15/15 Pct Recovery = 92% Analysis Date = 03/15/15 Pct Recovery = 92% Analysis Date = 03/10/15 Pct Recovery = 91% Analysis Date = 03/10/15 Pct Recovery = 91% Analysis Date = 03/05/15 Pct Recovery = 91% Analysis Date = 03/05/15 Pct Recovery = 91% Analysis Date = 02/28/15 Pct Recovery = 91% Analysis Date = 02/28/15 Pct Recovery = 91% Analysis Date = 02/23/15 Pct Recovery = 91% Analysis Date = 02/23/15 Pct Recovery = 91% Analysis Date = 02/19/15 Pct Recovery = 90% Analysis Date = 02/19/15 Pct Recovery = 90% Analysis Date = 02/14/15 Pct Recovery = 90% Analysis Date = 02/14/15 Pct Recovery = 90% Analysis Date = 02/09/15 Pct Recovery = 90% Analysis Date = 02/09/15 Pct Recovery = 90% Analysis Date = 02/04/15 Pct Recovery = 90% Analysis Date = 02/04/15 Pct Recovery = 90% Analysis Date = 01/31/15 Pct Recovery = 90% Analysis Date = 01/31/15 Pct Recovery = 90% Analysis Date = 01/26/15 Pct Recovery = 90% Analysis Date = 01/26/15 Pct Recovery = 90% Analysis Date = 01/21/15 Pct Recovery = 89% Analysis Date = 01/21/15 Pct Recovery = 89% Analysis Date = 01/16/15 Pct Recovery = 89% Analysis Date = 01/16/15 Pct Recovery = 89% Analysis Date = 01/11/15 Pct Recovery = 89% Analysis Date = 01/11/15 Pct Recovery = 89% Analysis Date = 01/07/15 Pct Recovery = 89% Analysis Date = 01/07/15 Pct Recovery = 89% Analysis Date = 01/02/15 Pct Recovery = 89% Analysis Date = 01/02/15 Pct Recovery = 89% Analysis Date = 12/28/14 Pct Recovery = 89% Analysis Date = 12/28/14 Pct Recovery = 89% Analysis Date = 12/23/14 Pct Recovery = 89% Analysis Date = 12/23/14 Pct Recovery = 89% Analysis Date = 12/18/14 Pct Recovery = 88% Analysis Date = 12/18/14 Pct Recovery = 88% Analysis Date = 12/14/14 Pct Recovery = 88% Analysis Date = 12/14/14 Pct Recovery = 88% Analysis Date = 12/09/14 Pct Recovery = 88% Analysis Date = 12/09/14 Pct Recovery = 88% Analysis Date = 12/04/14 Pct Recovery = 88% Analysis Date = 12/04/14 Pct Recovery = 88% Analysis Date = 11/29/14 Pct Recovery = 88% Analysis Date = 11/29/14 Pct Recovery = 88% Analysis Date = 11/24/14 Pct Recovery = 88% Analysis Date = 11/24/14 Pct Recovery = 88% Analysis Date = 11/20/14 Pct Recovery = 87% Analysis Date = 11/20/14 Pct Recovery = 87% Analysis Date = 11/15/14 Pct Recovery = 87% Analysis Date = 11/15/14 Pct Recovery = 87% Analysis Date = 11/10/14 Pct Recovery = 87% Analysis Date = 11/10/14 Pct Recovery = 87% Analysis Date = 11/05/14 Pct Recovery = 87% Analysis Date = 11/05/14 Pct Recovery = 87% Analysis Date = 11/01/14 Pct Recovery = 87% Analysis Date = 11/01/14 Pct Recovery = 87% Analysis Date = 10/27/14 Pct Recovery = 87% Analysis Date = 10/27/14 Pct Recovery = 87% Analysis Date = 10/22/14 Pct Recovery = 86% Analysis Date = 10/22/14 Pct Recovery = 86% Analysis Date = 10/17/14 Pct Recovery = 86% Analysis Date = 10/17/14 Pct Recovery = 86% Analysis Date = 10/12/14 Pct Recovery = 86% Analysis Date = 10/12/14 Pct Recovery = 86% Analysis Date = 10/08/14 Pct Recovery = 86% Analysis Date = 10/08/14 Pct Recovery = 86% Analysis Date = 10/03/14 Pct Recovery = 86% Analysis Date = 10/03/14 Pct Recovery = 86% Analysis Date = 09/28/14 Pct Recovery = 85% Analysis Date = 09/28/14 Pct Recovery = 85% Analysis Date = 09/23/14 Pct Recovery = 85% Analysis Date = 09/23/14 Pct Recovery = 85% Analysis Date = 09/18/14 Pct Recovery = 85% Analysis Date = 09/18/14 Pct Recovery = 85% Analysis Date = 09/14/14 Pct Recovery = 85% Analysis Date = 09/14/14 Pct Recovery = 85% Analysis Date = 09/09/14 Pct Recovery = 85% Analysis Date = 09/09/14 Pct Recovery = 85% Analysis Date = 09/04/14 Pct Recovery = 84% Analysis Date = 09/04/14 Pct Recovery = 84% Analysis Date = 08/30/14 Pct Recovery = 84% Analysis Date = 08/30/14 Pct Recovery = 84% Analysis Date = 08/25/14 Pct Recovery = 84% Analysis Date = 08/25/14 Pct Recovery = 84% Analysis Date = 08/21/14 Pct Recovery = 84% Analysis Date = 08/21/14 Pct Recovery = 84% Analysis Date = 08/16/14 Pct Recovery = 84% Analysis Date = 08/16/14 Pct Recovery = 84% Analysis Date = 08/11/14 Pct Recovery = 84% Analysis Date = 08/11/14 Pct Recovery = 84% Analysis Date = 08/06/14 Pct Recovery = 84% Analysis Date = 08/06/14 Pct Recovery = 84% Analysis Date = 08/02/14 Pct Recovery = 83% Analysis Date = 08/02/14 Pct Recovery = 83% Analysis Date = 07/28/14 Pct Recovery = 83% Analysis Date = 07/28/14 Pct Recovery = 83% Analysis Date = 07/23/14 Pct Recovery = 83% Analysis Date = 07/23/14 Pct Recovery = 83% Analysis Date = 07/18/14 Pct Recovery = 83% Analysis Date = 07/18/14 Pct Recovery = 83% Analysis Date = 07/13/14 Pct Recovery = 83% Analysis Date = 07/13/14 Pct Recovery = 83% Analysis Date = 07/09/14 Pct Recovery = 83% Analysis Date = 07/09/14 Pct Recovery = 83% Analysis Date = 07/04/14 Pct Recovery = 83% Analysis Date = 07/04/14 Pct Recovery = 83% Analysis Date = 06/29/14 Pct Recovery = 83% Analysis Date = 06/29/14 Pct Recovery = 83% Analysis Date = 06/24/14 Pct Recovery = 82% Analysis Date = 06/24/14 Pct Recovery = 82% Analysis Date = 06/19/14 Pct Recovery = 82% Analysis Date = 06/19/14 Pct Recovery = 82% Analysis Date = 06/15/14 Pct Recovery = 82% Analysis Date = 06/15/14 Pct Recovery = 82% Analysis Date = 06/10/14 Pct Recovery = 82% Analysis Date = 06/10/14 Pct Recovery = 82% Analysis Date = 06/05/14 Pct Recovery = 82% Analysis Date = 06/05/14 Pct Recovery = 82% Analysis Date = 05/31/14 Pct Recovery = 82% Analysis Date = 05/31/14 Pct Recovery = 82% Analysis Date = 05/26/14 Pct Recovery = 82% Analysis Date = 05/26/14 Pct Recovery = 82% Analysis Date = 05/22/14 Pct Recovery = 82% Analysis Date = 05/22/14 Pct Recovery = 82% Analysis Date = 05/17/14 Pct Recovery = 82% Analysis Date = 05/17/14 Pct Recovery = 82% Analysis Date = 05/12/14 Pct Recovery = 82% Analysis Date = 05/12/14 Pct Recovery = 82% Analysis Date = 05/07/14 Pct Recovery = 82% Analysis Date = 05/07/14 Pct Recovery = 82% Analysis Date = 05/03/14 Pct Recovery = 82% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
METHYL IODIDE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 48 94% 26% 95% 25%
Total 48 94% 26% 95% 25%

Sample Statistics
METHYL IODIDE

Characteristic N % % Basis
Plotted 48 100% Spiked
Estimated Values 48 100% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 48 .  
False Negatives 0 0% 0 out of 48
Not Spiked 25 .  
False Positives 12 48% 12 out of 25

BQS OBSP Determination:
METHYL METHACRYLATE
METHOD: 4440 , TESTIDCODE: 81597GCM66
Open Data Set

Analysis Date = 12/12/16 SpikeMix = Accu 216041125: 40 µl & Crescent 03FF058: 40 µl Pct Recovery = 95% Analysis Date = 07/20/16 SpikeMix = Supelco LC20141V: 40 µl & Accu 216041125: 40 µl Pct Recovery = 96% Analysis Date = 07/14/16 SpikeMix = Accu 216041125: 40 µl & NSI 041816AVOC: 40 µl Pct Recovery = 79% Analysis Date = 08/12/16 SpikeMix = ChemService 5082900: 25 µl & Phenova B20160319: 25 µl Pct Recovery = 87% Analysis Date = 06/21/16 SpikeMix = Phenova B20160319: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 93% Analysis Date = 09/08/16 SpikeMix = Supelco LC20141V: 25 µl & Accu 216041125: 25 µl Pct Recovery = 79% Analysis Date = 05/24/16 SpikeMix = Accu 216041125: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 90% Analysis Date = 09/29/15 SpikeMix = Accu 215041380: 25 µl & ERA 0406-15-03: 25 µl Pct Recovery = 85% Analysis Date = 08/15/15 SpikeMix = Supelco LC13545: 25 µl & Crescent 04EE008: 25 µl Pct Recovery = 89% Analysis Date = 07/13/15 SpikeMix = Crescent 04EE008: 25 µl & NSI 050515AVOC: 25 µl Pct Recovery = 92% Analysis Date = 11/29/16 SpikeMix = ChemService 5082900: 15 µl & Phenova B20160319: 15 µl Pct Recovery = 84% Analysis Date = 09/08/16 SpikeMix = Phenova B20160319: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 85% Analysis Date = 07/29/16 SpikeMix = Phenova B20160319: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 89% Analysis Date = 05/27/16 SpikeMix = Phenova B20160319: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 88% Analysis Date = 10/13/16 SpikeMix = Accu 216041125: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 101% Analysis Date = 08/20/16 SpikeMix = Accu 216041125: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 104% Analysis Date = 06/30/16 SpikeMix = ChemService 5082900: 15 µl & Accu 216041125: 15 µl Pct Recovery = 70% Analysis Date = 04/09/15 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 86% Analysis Date = 03/06/15 SpikeMix = ERA 0227-14-06.1A: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 90% Analysis Date = 11/14/14 SpikeMix = Crescent 03DD004: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 99% Analysis Date = 08/16/14 SpikeMix = ERA 0227-14-06.1A: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 90% Analysis Date = 07/01/14 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 90% Analysis Date = 11/22/14 SpikeMix = NSI 032614: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 93% Analysis Date = 06/10/14 SpikeMix = Crescent 03DD004: 20 µl & NSI 032614: 20 µl Pct Recovery = 95% Analysis Date = 06/10/14 SpikeMix = NSI 032614: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 93% Analysis Date = 05/01/14 SpikeMix = Accu 214031115: 20 µl & NSI 032614: 20 µl Pct Recovery = 97% Analysis Date = 04/02/16 SpikeMix = Supelco LC13545: 15 µl & Accu 215041380: 15 µl Pct Recovery = 83% Analysis Date = 03/04/16 SpikeMix = Accu 215041380: 15 µl & ERA 0406-15-03: 15 µl Pct Recovery = 85% Analysis Date = 06/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Accu 215041380: 15 µl Pct Recovery = 85% Analysis Date = 12/18/15 SpikeMix = Supelco LC13545: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 105% Analysis Date = 10/17/15 SpikeMix = Crescent 04EE008: 15 µl & NSI 050515AVOC: 15 µl Pct Recovery = 94% Analysis Date = 05/09/15 SpikeMix = Spex Organics EN150428007: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 91% Analysis Date = 02/18/16 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 86% Analysis Date = 11/20/15 SpikeMix = Accu 215041380: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 96% Analysis Date = 11/12/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 90% Analysis Date = 05/21/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 97% Analysis Date = 05/13/16 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 96% Analysis Date = 01/27/16 SpikeMix = Crescent 04EE008: 10 µl & NSI 050515AVOC: 10 µl Pct Recovery = 85% Analysis Date = 08/07/15 SpikeMix = Crescent 04EE008: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 95% Analysis Date = 05/09/15 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 81% Analysis Date = 01/13/15 SpikeMix = Accu 214031115: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 92% Analysis Date = 10/21/14 SpikeMix = ERA 0227-14-06.1A: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 94% Analysis Date = 10/04/14 SpikeMix = Crescent 03DD004: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 91% Analysis Date = 07/11/14 SpikeMix = Spex Organics C1140417015: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 103% Analysis Date = 09/09/14 SpikeMix = Accu 214031115: 10 µl & NSI 032614: 10 µl Pct Recovery = 117% Analysis Date = 09/09/14 SpikeMix = NSI 032614: 10 µl & Spex Organics C1140417015: 10 µl Pct Recovery = 114% Analysis Date = 07/29/14 SpikeMix = Crescent 03DD004: 10 µl & NSI 032614: 10 µl Pct Recovery = 107% Analysis Date = 05/30/14 SpikeMix = NSI 032614: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 82% Analysis Date = 12/11/16 Pct Recovery = 89% Analysis Date = 12/07/16 Pct Recovery = 89% Analysis Date = 12/07/16 Pct Recovery = 89% Analysis Date = 12/02/16 Pct Recovery = 89% Analysis Date = 12/02/16 Pct Recovery = 89% Analysis Date = 11/27/16 Pct Recovery = 89% Analysis Date = 11/27/16 Pct Recovery = 89% Analysis Date = 11/22/16 Pct Recovery = 89% Analysis Date = 11/22/16 Pct Recovery = 89% Analysis Date = 11/18/16 Pct Recovery = 89% Analysis Date = 11/18/16 Pct Recovery = 89% Analysis Date = 11/13/16 Pct Recovery = 89% Analysis Date = 11/13/16 Pct Recovery = 89% Analysis Date = 11/08/16 Pct Recovery = 89% Analysis Date = 11/08/16 Pct Recovery = 89% Analysis Date = 11/03/16 Pct Recovery = 89% Analysis Date = 11/03/16 Pct Recovery = 89% Analysis Date = 10/29/16 Pct Recovery = 89% Analysis Date = 10/29/16 Pct Recovery = 89% Analysis Date = 10/25/16 Pct Recovery = 89% Analysis Date = 10/25/16 Pct Recovery = 89% Analysis Date = 10/20/16 Pct Recovery = 89% Analysis Date = 10/20/16 Pct Recovery = 89% Analysis Date = 10/15/16 Pct Recovery = 89% Analysis Date = 10/15/16 Pct Recovery = 89% Analysis Date = 10/10/16 Pct Recovery = 89% Analysis Date = 10/10/16 Pct Recovery = 89% Analysis Date = 10/06/16 Pct Recovery = 89% Analysis Date = 10/06/16 Pct Recovery = 89% Analysis Date = 10/01/16 Pct Recovery = 89% Analysis Date = 10/01/16 Pct Recovery = 89% Analysis Date = 09/26/16 Pct Recovery = 89% Analysis Date = 09/26/16 Pct Recovery = 89% Analysis Date = 09/21/16 Pct Recovery = 89% Analysis Date = 09/21/16 Pct Recovery = 89% Analysis Date = 09/16/16 Pct Recovery = 89% Analysis Date = 09/16/16 Pct Recovery = 89% Analysis Date = 09/12/16 Pct Recovery = 89% Analysis Date = 09/12/16 Pct Recovery = 89% Analysis Date = 09/07/16 Pct Recovery = 89% Analysis Date = 09/07/16 Pct Recovery = 89% Analysis Date = 09/02/16 Pct Recovery = 89% Analysis Date = 09/02/16 Pct Recovery = 89% Analysis Date = 08/28/16 Pct Recovery = 89% Analysis Date = 08/28/16 Pct Recovery = 89% Analysis Date = 08/24/16 Pct Recovery = 89% Analysis Date = 08/24/16 Pct Recovery = 89% Analysis Date = 08/19/16 Pct Recovery = 89% Analysis Date = 08/19/16 Pct Recovery = 89% Analysis Date = 08/14/16 Pct Recovery = 89% Analysis Date = 08/14/16 Pct Recovery = 89% Analysis Date = 08/09/16 Pct Recovery = 89% Analysis Date = 08/09/16 Pct Recovery = 89% Analysis Date = 08/04/16 Pct Recovery = 89% Analysis Date = 08/04/16 Pct Recovery = 89% Analysis Date = 07/31/16 Pct Recovery = 89% Analysis Date = 07/31/16 Pct Recovery = 89% Analysis Date = 07/26/16 Pct Recovery = 89% Analysis Date = 07/26/16 Pct Recovery = 89% Analysis Date = 07/21/16 Pct Recovery = 89% Analysis Date = 07/21/16 Pct Recovery = 89% Analysis Date = 07/16/16 Pct Recovery = 89% Analysis Date = 07/16/16 Pct Recovery = 89% Analysis Date = 07/12/16 Pct Recovery = 89% Analysis Date = 07/12/16 Pct Recovery = 89% Analysis Date = 07/07/16 Pct Recovery = 89% Analysis Date = 07/07/16 Pct Recovery = 89% Analysis Date = 07/02/16 Pct Recovery = 89% Analysis Date = 07/02/16 Pct Recovery = 89% Analysis Date = 06/27/16 Pct Recovery = 89% Analysis Date = 06/27/16 Pct Recovery = 89% Analysis Date = 06/22/16 Pct Recovery = 89% Analysis Date = 06/22/16 Pct Recovery = 89% Analysis Date = 06/18/16 Pct Recovery = 89% Analysis Date = 06/18/16 Pct Recovery = 89% Analysis Date = 06/13/16 Pct Recovery = 89% Analysis Date = 06/13/16 Pct Recovery = 89% Analysis Date = 06/08/16 Pct Recovery = 89% Analysis Date = 06/08/16 Pct Recovery = 89% Analysis Date = 06/03/16 Pct Recovery = 89% Analysis Date = 06/03/16 Pct Recovery = 89% Analysis Date = 05/30/16 Pct Recovery = 89% Analysis Date = 05/30/16 Pct Recovery = 89% Analysis Date = 05/25/16 Pct Recovery = 89% Analysis Date = 05/25/16 Pct Recovery = 89% Analysis Date = 05/20/16 Pct Recovery = 89% Analysis Date = 05/20/16 Pct Recovery = 89% Analysis Date = 05/15/16 Pct Recovery = 89% Analysis Date = 05/15/16 Pct Recovery = 89% Analysis Date = 05/10/16 Pct Recovery = 89% Analysis Date = 05/10/16 Pct Recovery = 89% Analysis Date = 05/06/16 Pct Recovery = 89% Analysis Date = 05/06/16 Pct Recovery = 89% Analysis Date = 05/01/16 Pct Recovery = 89% Analysis Date = 05/01/16 Pct Recovery = 89% Analysis Date = 04/26/16 Pct Recovery = 89% Analysis Date = 04/26/16 Pct Recovery = 89% Analysis Date = 04/21/16 Pct Recovery = 89% Analysis Date = 04/21/16 Pct Recovery = 89% Analysis Date = 04/16/16 Pct Recovery = 89% Analysis Date = 04/16/16 Pct Recovery = 89% Analysis Date = 04/12/16 Pct Recovery = 89% Analysis Date = 04/12/16 Pct Recovery = 89% Analysis Date = 04/07/16 Pct Recovery = 89% Analysis Date = 04/07/16 Pct Recovery = 89% Analysis Date = 04/02/16 Pct Recovery = 89% Analysis Date = 04/02/16 Pct Recovery = 89% Analysis Date = 03/28/16 Pct Recovery = 89% Analysis Date = 03/28/16 Pct Recovery = 89% Analysis Date = 03/24/16 Pct Recovery = 89% Analysis Date = 03/24/16 Pct Recovery = 89% Analysis Date = 03/19/16 Pct Recovery = 89% Analysis Date = 03/19/16 Pct Recovery = 89% Analysis Date = 03/14/16 Pct Recovery = 90% Analysis Date = 03/14/16 Pct Recovery = 90% Analysis Date = 03/09/16 Pct Recovery = 90% Analysis Date = 03/09/16 Pct Recovery = 90% Analysis Date = 03/04/16 Pct Recovery = 90% Analysis Date = 03/04/16 Pct Recovery = 90% Analysis Date = 02/29/16 Pct Recovery = 90% Analysis Date = 02/29/16 Pct Recovery = 90% Analysis Date = 02/24/16 Pct Recovery = 90% Analysis Date = 02/24/16 Pct Recovery = 90% Analysis Date = 02/19/16 Pct Recovery = 90% Analysis Date = 02/19/16 Pct Recovery = 90% Analysis Date = 02/14/16 Pct Recovery = 90% Analysis Date = 02/14/16 Pct Recovery = 90% Analysis Date = 02/10/16 Pct Recovery = 90% Analysis Date = 02/10/16 Pct Recovery = 90% Analysis Date = 02/05/16 Pct Recovery = 90% Analysis Date = 02/05/16 Pct Recovery = 90% Analysis Date = 01/31/16 Pct Recovery = 90% Analysis Date = 01/31/16 Pct Recovery = 90% Analysis Date = 01/26/16 Pct Recovery = 90% Analysis Date = 01/26/16 Pct Recovery = 90% Analysis Date = 01/21/16 Pct Recovery = 90% Analysis Date = 01/21/16 Pct Recovery = 90% Analysis Date = 01/17/16 Pct Recovery = 90% Analysis Date = 01/17/16 Pct Recovery = 90% Analysis Date = 01/12/16 Pct Recovery = 90% Analysis Date = 01/12/16 Pct Recovery = 90% Analysis Date = 01/07/16 Pct Recovery = 90% Analysis Date = 01/07/16 Pct Recovery = 90% Analysis Date = 01/02/16 Pct Recovery = 90% Analysis Date = 01/02/16 Pct Recovery = 90% Analysis Date = 12/29/15 Pct Recovery = 90% Analysis Date = 12/29/15 Pct Recovery = 90% Analysis Date = 12/24/15 Pct Recovery = 90% Analysis Date = 12/24/15 Pct Recovery = 90% Analysis Date = 12/19/15 Pct Recovery = 90% Analysis Date = 12/19/15 Pct Recovery = 90% Analysis Date = 12/14/15 Pct Recovery = 90% Analysis Date = 12/14/15 Pct Recovery = 90% Analysis Date = 12/09/15 Pct Recovery = 90% Analysis Date = 12/09/15 Pct Recovery = 90% Analysis Date = 12/05/15 Pct Recovery = 90% Analysis Date = 12/05/15 Pct Recovery = 90% Analysis Date = 11/30/15 Pct Recovery = 90% Analysis Date = 11/30/15 Pct Recovery = 90% Analysis Date = 11/25/15 Pct Recovery = 90% Analysis Date = 11/25/15 Pct Recovery = 90% Analysis Date = 11/20/15 Pct Recovery = 90% Analysis Date = 11/20/15 Pct Recovery = 90% Analysis Date = 11/16/15 Pct Recovery = 90% Analysis Date = 11/16/15 Pct Recovery = 90% Analysis Date = 11/11/15 Pct Recovery = 90% Analysis Date = 11/11/15 Pct Recovery = 90% Analysis Date = 11/06/15 Pct Recovery = 90% Analysis Date = 11/06/15 Pct Recovery = 90% Analysis Date = 11/01/15 Pct Recovery = 90% Analysis Date = 11/01/15 Pct Recovery = 90% Analysis Date = 10/27/15 Pct Recovery = 90% Analysis Date = 10/27/15 Pct Recovery = 90% Analysis Date = 10/23/15 Pct Recovery = 90% Analysis Date = 10/23/15 Pct Recovery = 90% Analysis Date = 10/18/15 Pct Recovery = 90% Analysis Date = 10/18/15 Pct Recovery = 90% Analysis Date = 10/13/15 Pct Recovery = 90% Analysis Date = 10/13/15 Pct Recovery = 90% Analysis Date = 10/08/15 Pct Recovery = 90% Analysis Date = 10/08/15 Pct Recovery = 90% Analysis Date = 10/04/15 Pct Recovery = 90% Analysis Date = 10/04/15 Pct Recovery = 90% Analysis Date = 09/29/15 Pct Recovery = 90% Analysis Date = 09/29/15 Pct Recovery = 90% Analysis Date = 09/24/15 Pct Recovery = 90% Analysis Date = 09/24/15 Pct Recovery = 90% Analysis Date = 09/19/15 Pct Recovery = 90% Analysis Date = 09/19/15 Pct Recovery = 90% Analysis Date = 09/14/15 Pct Recovery = 90% Analysis Date = 09/14/15 Pct Recovery = 90% Analysis Date = 09/10/15 Pct Recovery = 90% Analysis Date = 09/10/15 Pct Recovery = 90% Analysis Date = 09/05/15 Pct Recovery = 90% Analysis Date = 09/05/15 Pct Recovery = 90% Analysis Date = 08/31/15 Pct Recovery = 90% Analysis Date = 08/31/15 Pct Recovery = 90% Analysis Date = 08/26/15 Pct Recovery = 90% Analysis Date = 08/26/15 Pct Recovery = 90% Analysis Date = 08/21/15 Pct Recovery = 90% Analysis Date = 08/21/15 Pct Recovery = 90% Analysis Date = 08/17/15 Pct Recovery = 90% Analysis Date = 08/17/15 Pct Recovery = 90% Analysis Date = 08/12/15 Pct Recovery = 90% Analysis Date = 08/12/15 Pct Recovery = 90% Analysis Date = 08/07/15 Pct Recovery = 91% Analysis Date = 08/07/15 Pct Recovery = 91% Analysis Date = 08/02/15 Pct Recovery = 91% Analysis Date = 08/02/15 Pct Recovery = 91% Analysis Date = 07/29/15 Pct Recovery = 91% Analysis Date = 07/29/15 Pct Recovery = 91% Analysis Date = 07/24/15 Pct Recovery = 91% Analysis Date = 07/24/15 Pct Recovery = 91% Analysis Date = 07/19/15 Pct Recovery = 91% Analysis Date = 07/19/15 Pct Recovery = 91% Analysis Date = 07/14/15 Pct Recovery = 91% Analysis Date = 07/14/15 Pct Recovery = 91% Analysis Date = 07/09/15 Pct Recovery = 91% Analysis Date = 07/09/15 Pct Recovery = 91% Analysis Date = 07/05/15 Pct Recovery = 91% Analysis Date = 07/05/15 Pct Recovery = 91% Analysis Date = 06/30/15 Pct Recovery = 91% Analysis Date = 06/30/15 Pct Recovery = 91% Analysis Date = 06/25/15 Pct Recovery = 91% Analysis Date = 06/25/15 Pct Recovery = 91% Analysis Date = 06/20/15 Pct Recovery = 91% Analysis Date = 06/20/15 Pct Recovery = 91% Analysis Date = 06/16/15 Pct Recovery = 91% Analysis Date = 06/16/15 Pct Recovery = 91% Analysis Date = 06/11/15 Pct Recovery = 91% Analysis Date = 06/11/15 Pct Recovery = 91% Analysis Date = 06/06/15 Pct Recovery = 91% Analysis Date = 06/06/15 Pct Recovery = 91% Analysis Date = 06/01/15 Pct Recovery = 91% Analysis Date = 06/01/15 Pct Recovery = 91% Analysis Date = 05/27/15 Pct Recovery = 91% Analysis Date = 05/27/15 Pct Recovery = 91% Analysis Date = 05/23/15 Pct Recovery = 91% Analysis Date = 05/23/15 Pct Recovery = 91% Analysis Date = 05/18/15 Pct Recovery = 91% Analysis Date = 05/18/15 Pct Recovery = 91% Analysis Date = 05/13/15 Pct Recovery = 91% Analysis Date = 05/13/15 Pct Recovery = 91% Analysis Date = 05/08/15 Pct Recovery = 91% Analysis Date = 05/08/15 Pct Recovery = 91% Analysis Date = 05/04/15 Pct Recovery = 92% Analysis Date = 05/04/15 Pct Recovery = 92% Analysis Date = 04/29/15 Pct Recovery = 92% Analysis Date = 04/29/15 Pct Recovery = 92% Analysis Date = 04/24/15 Pct Recovery = 92% Analysis Date = 04/24/15 Pct Recovery = 92% Analysis Date = 04/19/15 Pct Recovery = 92% Analysis Date = 04/19/15 Pct Recovery = 92% Analysis Date = 04/14/15 Pct Recovery = 92% Analysis Date = 04/14/15 Pct Recovery = 92% Analysis Date = 04/10/15 Pct Recovery = 92% Analysis Date = 04/10/15 Pct Recovery = 92% Analysis Date = 04/05/15 Pct Recovery = 92% Analysis Date = 04/05/15 Pct Recovery = 92% Analysis Date = 03/31/15 Pct Recovery = 92% Analysis Date = 03/31/15 Pct Recovery = 92% Analysis Date = 03/26/15 Pct Recovery = 92% Analysis Date = 03/26/15 Pct Recovery = 92% Analysis Date = 03/22/15 Pct Recovery = 92% Analysis Date = 03/22/15 Pct Recovery = 92% Analysis Date = 03/17/15 Pct Recovery = 93% Analysis Date = 03/17/15 Pct Recovery = 93% Analysis Date = 03/12/15 Pct Recovery = 93% Analysis Date = 03/12/15 Pct Recovery = 93% Analysis Date = 03/07/15 Pct Recovery = 93% Analysis Date = 03/07/15 Pct Recovery = 93% Analysis Date = 03/02/15 Pct Recovery = 93% Analysis Date = 03/02/15 Pct Recovery = 93% Analysis Date = 02/26/15 Pct Recovery = 93% Analysis Date = 02/26/15 Pct Recovery = 93% Analysis Date = 02/21/15 Pct Recovery = 93% Analysis Date = 02/21/15 Pct Recovery = 93% Analysis Date = 02/16/15 Pct Recovery = 93% Analysis Date = 02/16/15 Pct Recovery = 93% Analysis Date = 02/11/15 Pct Recovery = 93% Analysis Date = 02/11/15 Pct Recovery = 93% Analysis Date = 02/07/15 Pct Recovery = 93% Analysis Date = 02/07/15 Pct Recovery = 93% Analysis Date = 02/02/15 Pct Recovery = 94% Analysis Date = 02/02/15 Pct Recovery = 94% Analysis Date = 01/28/15 Pct Recovery = 94% Analysis Date = 01/28/15 Pct Recovery = 94% Analysis Date = 01/23/15 Pct Recovery = 94% Analysis Date = 01/23/15 Pct Recovery = 94% Analysis Date = 01/18/15 Pct Recovery = 94% Analysis Date = 01/18/15 Pct Recovery = 94% Analysis Date = 01/14/15 Pct Recovery = 94% Analysis Date = 01/14/15 Pct Recovery = 94% Analysis Date = 01/09/15 Pct Recovery = 94% Analysis Date = 01/09/15 Pct Recovery = 94% Analysis Date = 01/04/15 Pct Recovery = 94% Analysis Date = 01/04/15 Pct Recovery = 94% Analysis Date = 12/30/14 Pct Recovery = 94% Analysis Date = 12/30/14 Pct Recovery = 94% Analysis Date = 12/25/14 Pct Recovery = 94% Analysis Date = 12/25/14 Pct Recovery = 94% Analysis Date = 12/21/14 Pct Recovery = 94% Analysis Date = 12/21/14 Pct Recovery = 94% Analysis Date = 12/16/14 Pct Recovery = 94% Analysis Date = 12/16/14 Pct Recovery = 94% Analysis Date = 12/11/14 Pct Recovery = 95% Analysis Date = 12/11/14 Pct Recovery = 95% Analysis Date = 12/06/14 Pct Recovery = 95% Analysis Date = 12/06/14 Pct Recovery = 95% Analysis Date = 12/02/14 Pct Recovery = 95% Analysis Date = 12/02/14 Pct Recovery = 95% Analysis Date = 11/27/14 Pct Recovery = 95% Analysis Date = 11/27/14 Pct Recovery = 95% Analysis Date = 11/22/14 Pct Recovery = 95% Analysis Date = 11/22/14 Pct Recovery = 95% Analysis Date = 11/17/14 Pct Recovery = 95% Analysis Date = 11/17/14 Pct Recovery = 95% Analysis Date = 11/12/14 Pct Recovery = 95% Analysis Date = 11/12/14 Pct Recovery = 95% Analysis Date = 11/08/14 Pct Recovery = 95% Analysis Date = 11/08/14 Pct Recovery = 95% Analysis Date = 11/03/14 Pct Recovery = 95% Analysis Date = 11/03/14 Pct Recovery = 95% Analysis Date = 10/29/14 Pct Recovery = 95% Analysis Date = 10/29/14 Pct Recovery = 95% Analysis Date = 10/24/14 Pct Recovery = 95% Analysis Date = 10/24/14 Pct Recovery = 95% Analysis Date = 10/20/14 Pct Recovery = 95% Analysis Date = 10/20/14 Pct Recovery = 95% Analysis Date = 10/15/14 Pct Recovery = 95% Analysis Date = 10/15/14 Pct Recovery = 95% Analysis Date = 10/10/14 Pct Recovery = 96% Analysis Date = 10/10/14 Pct Recovery = 96% Analysis Date = 10/05/14 Pct Recovery = 96% Analysis Date = 10/05/14 Pct Recovery = 96% Analysis Date = 09/30/14 Pct Recovery = 96% Analysis Date = 09/30/14 Pct Recovery = 96% Analysis Date = 09/26/14 Pct Recovery = 96% Analysis Date = 09/26/14 Pct Recovery = 96% Analysis Date = 09/21/14 Pct Recovery = 96% Analysis Date = 09/21/14 Pct Recovery = 96% Analysis Date = 09/16/14 Pct Recovery = 96% Analysis Date = 09/16/14 Pct Recovery = 96% Analysis Date = 09/11/14 Pct Recovery = 96% Analysis Date = 09/11/14 Pct Recovery = 96% Analysis Date = 09/07/14 Pct Recovery = 96% Analysis Date = 09/07/14 Pct Recovery = 96% Analysis Date = 09/02/14 Pct Recovery = 96% Analysis Date = 09/02/14 Pct Recovery = 96% Analysis Date = 08/28/14 Pct Recovery = 96% Analysis Date = 08/28/14 Pct Recovery = 96% Analysis Date = 08/23/14 Pct Recovery = 96% Analysis Date = 08/23/14 Pct Recovery = 96% Analysis Date = 08/18/14 Pct Recovery = 96% Analysis Date = 08/18/14 Pct Recovery = 96% Analysis Date = 08/14/14 Pct Recovery = 97% Analysis Date = 08/14/14 Pct Recovery = 97% Analysis Date = 08/09/14 Pct Recovery = 97% Analysis Date = 08/09/14 Pct Recovery = 97% Analysis Date = 08/04/14 Pct Recovery = 97% Analysis Date = 08/04/14 Pct Recovery = 97% Analysis Date = 07/30/14 Pct Recovery = 97% Analysis Date = 07/30/14 Pct Recovery = 97% Analysis Date = 07/26/14 Pct Recovery = 97% Analysis Date = 07/26/14 Pct Recovery = 97% Analysis Date = 07/21/14 Pct Recovery = 97% Analysis Date = 07/21/14 Pct Recovery = 97% Analysis Date = 07/16/14 Pct Recovery = 97% Analysis Date = 07/16/14 Pct Recovery = 97% Analysis Date = 07/11/14 Pct Recovery = 97% Analysis Date = 07/11/14 Pct Recovery = 97% Analysis Date = 07/06/14 Pct Recovery = 97% Analysis Date = 07/06/14 Pct Recovery = 97% Analysis Date = 07/02/14 Pct Recovery = 97% Analysis Date = 07/02/14 Pct Recovery = 97% Analysis Date = 06/27/14 Pct Recovery = 97% Analysis Date = 06/27/14 Pct Recovery = 97% Analysis Date = 06/22/14 Pct Recovery = 97% Analysis Date = 06/22/14 Pct Recovery = 97% Analysis Date = 06/17/14 Pct Recovery = 98% Analysis Date = 06/17/14 Pct Recovery = 98% Analysis Date = 06/13/14 Pct Recovery = 98% Analysis Date = 06/13/14 Pct Recovery = 98% Analysis Date = 06/08/14 Pct Recovery = 98% Analysis Date = 06/08/14 Pct Recovery = 98% Analysis Date = 06/03/14 Pct Recovery = 98% Analysis Date = 06/03/14 Pct Recovery = 98% Analysis Date = 05/29/14 Pct Recovery = 98% Analysis Date = 05/29/14 Pct Recovery = 98% Analysis Date = 05/24/14 Pct Recovery = 98% Analysis Date = 05/24/14 Pct Recovery = 98% Analysis Date = 05/20/14 Pct Recovery = 98% Analysis Date = 05/20/14 Pct Recovery = 98% Analysis Date = 05/15/14 Pct Recovery = 98% Analysis Date = 05/15/14 Pct Recovery = 98% Analysis Date = 05/10/14 Pct Recovery = 98% Analysis Date = 05/10/14 Pct Recovery = 98% Analysis Date = 05/05/14 Pct Recovery = 98% Analysis Date = 05/05/14 Pct Recovery = 98% Analysis Date = 05/01/14 Pct Recovery = 98% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
METHYL METHACRYLATE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 48 92% 9% 91% 8%
Total 48 92% 9% 91% 8%

Sample Statistics
METHYL METHACRYLATE

Characteristic N % % Basis
Plotted 48 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 48 .  
False Negatives 0 0% 0 out of 48
Not Spiked 25 .  
False Positives 0 0% 0 out of 25

BQS OBSP Determination:
N-PENTANE
METHOD: 4440 , TESTIDCODE: 81604GCM66
Open Data Set

Analysis Date = 12/16/16 SpikeMix = NSI 041816AVOC: 40 µl & ChemService 5082900: 40 µl Pct Recovery = 117% Analysis Date = 08/04/16 SpikeMix = Crescent 03FF058: 40 µl & Supelco LC20141V: 40 µl Pct Recovery = 111% Analysis Date = 07/20/16 SpikeMix = Supelco LC20141V: 40 µl & Accu 216041125: 40 µl Pct Recovery = 124% Analysis Date = 11/21/16 SpikeMix = Crescent 03FF058: 25 µl & Supelco LC20141V: 25 µl Pct Recovery = 87% Analysis Date = 09/08/16 SpikeMix = Supelco LC20141V: 25 µl & Accu 216041125: 25 µl Pct Recovery = 105% Analysis Date = 08/26/16 SpikeMix = NSI 041816AVOC: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 111% Analysis Date = 08/12/16 SpikeMix = ChemService 5082900: 25 µl & Phenova B20160319: 25 µl Pct Recovery = 110% Analysis Date = 06/30/16 SpikeMix = Crescent 03FF058: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 94% Analysis Date = 03/19/15 SpikeMix = Spex Organics C1140417015: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 52% Analysis Date = 12/17/14 SpikeMix = Supelco LC06438: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 45% Analysis Date = 11/14/14 SpikeMix = Crescent 03DD004: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 49% Analysis Date = 06/10/14 SpikeMix = Crescent 03DD004: 20 µl & NSI 032614: 20 µl Pct Recovery = 54% Analysis Date = 08/15/15 SpikeMix = Supelco LC13545: 25 µl & Crescent 04EE008: 25 µl Pct Recovery = 112% Analysis Date = 06/16/15 SpikeMix = ERA 0406-15-03: 25 µl & Supelco LC13545: 25 µl Pct Recovery = 102% Analysis Date = 04/09/15 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 72% Analysis Date = 08/19/14 SpikeMix = Spex Organics C1140417015: 20 µl & Accu 214031115: 20 µl Pct Recovery = 127% Analysis Date = 07/01/14 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 131% Analysis Date = 05/01/14 SpikeMix = Accu 214031115: 20 µl & NSI 032614: 20 µl Pct Recovery = 102% Analysis Date = 09/28/16 SpikeMix = Crescent 03FF058: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 106% Analysis Date = 06/30/16 SpikeMix = ChemService 5082900: 15 µl & Accu 216041125: 15 µl Pct Recovery = 102% Analysis Date = 06/10/16 SpikeMix = NSI 041816AVOC: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 146% Analysis Date = 05/27/16 SpikeMix = Phenova B20160319: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 99% Analysis Date = 04/26/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 95% Analysis Date = 02/05/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 113% Analysis Date = 11/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 118% Analysis Date = 10/16/15 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 103% Analysis Date = 05/09/15 SpikeMix = Spex Organics EN150428007: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 88% Analysis Date = 04/02/16 SpikeMix = Supelco LC13545: 15 µl & Accu 215041380: 15 µl Pct Recovery = 103% Analysis Date = 12/18/15 SpikeMix = Supelco LC13545: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 105% Analysis Date = 11/06/14 SpikeMix = Spex Organics C1140417015: 10 µl & Crescent 03DD004: 10 µl Pct Recovery = 48% Analysis Date = 10/04/14 SpikeMix = Crescent 03DD004: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 52% Analysis Date = 07/29/14 SpikeMix = Crescent 03DD004: 10 µl & NSI 032614: 10 µl Pct Recovery = 61% Analysis Date = 05/03/14 SpikeMix = Crescent 03DD004: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 72% Analysis Date = 01/13/15 SpikeMix = Accu 214031115: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 99% Analysis Date = 09/09/14 SpikeMix = Accu 214031115: 10 µl & NSI 032614: 10 µl Pct Recovery = 146% Analysis Date = 07/23/14 SpikeMix = Spex Organics C1140417015: 10 µl & Accu 214031115: 10 µl Pct Recovery = 143% Analysis Date = 06/18/14 SpikeMix = Supelco LC06438: 10 µl & Accu 214031115: 10 µl Pct Recovery = 130% Analysis Date = 02/18/16 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 118% Analysis Date = 11/12/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 116% Analysis Date = 09/03/15 SpikeMix = NSI 050515AVOC: 10 µl & Spex Organics EN150428007: 10 µl Pct Recovery = 104% Analysis Date = 05/21/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 83% Analysis Date = 05/13/16 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 84% Analysis Date = 03/17/16 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 117% Analysis Date = 12/10/15 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 128% Analysis Date = 06/27/15 SpikeMix = ERA 0406-15-03: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 102% Analysis Date = 05/09/15 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 73% Analysis Date = 11/29/16 SpikeMix = ChemService 5082900: 15 µl & Phenova B20160319: 15 µl Pct Recovery = 104% Analysis Date = 10/13/16 SpikeMix = NSI 041816AVOC: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 120% Analysis Date = 12/15/16 Pct Recovery = 106% Analysis Date = 12/11/16 Pct Recovery = 106% Analysis Date = 12/11/16 Pct Recovery = 106% Analysis Date = 12/06/16 Pct Recovery = 107% Analysis Date = 12/06/16 Pct Recovery = 107% Analysis Date = 12/01/16 Pct Recovery = 107% Analysis Date = 12/01/16 Pct Recovery = 107% Analysis Date = 11/26/16 Pct Recovery = 107% Analysis Date = 11/26/16 Pct Recovery = 107% Analysis Date = 11/21/16 Pct Recovery = 107% Analysis Date = 11/21/16 Pct Recovery = 107% Analysis Date = 11/17/16 Pct Recovery = 107% Analysis Date = 11/17/16 Pct Recovery = 107% Analysis Date = 11/12/16 Pct Recovery = 107% Analysis Date = 11/12/16 Pct Recovery = 107% Analysis Date = 11/07/16 Pct Recovery = 107% Analysis Date = 11/07/16 Pct Recovery = 107% Analysis Date = 11/02/16 Pct Recovery = 107% Analysis Date = 11/02/16 Pct Recovery = 107% Analysis Date = 10/28/16 Pct Recovery = 107% Analysis Date = 10/28/16 Pct Recovery = 107% Analysis Date = 10/24/16 Pct Recovery = 107% Analysis Date = 10/24/16 Pct Recovery = 107% Analysis Date = 10/19/16 Pct Recovery = 107% Analysis Date = 10/19/16 Pct Recovery = 107% Analysis Date = 10/14/16 Pct Recovery = 107% Analysis Date = 10/14/16 Pct Recovery = 107% Analysis Date = 10/09/16 Pct Recovery = 107% Analysis Date = 10/09/16 Pct Recovery = 107% Analysis Date = 10/04/16 Pct Recovery = 107% Analysis Date = 10/04/16 Pct Recovery = 107% Analysis Date = 09/30/16 Pct Recovery = 107% Analysis Date = 09/30/16 Pct Recovery = 107% Analysis Date = 09/25/16 Pct Recovery = 107% Analysis Date = 09/25/16 Pct Recovery = 107% Analysis Date = 09/20/16 Pct Recovery = 107% Analysis Date = 09/20/16 Pct Recovery = 107% Analysis Date = 09/15/16 Pct Recovery = 108% Analysis Date = 09/15/16 Pct Recovery = 108% Analysis Date = 09/10/16 Pct Recovery = 108% Analysis Date = 09/10/16 Pct Recovery = 108% Analysis Date = 09/06/16 Pct Recovery = 108% Analysis Date = 09/06/16 Pct Recovery = 108% Analysis Date = 09/01/16 Pct Recovery = 108% Analysis Date = 09/01/16 Pct Recovery = 108% Analysis Date = 08/27/16 Pct Recovery = 108% Analysis Date = 08/27/16 Pct Recovery = 108% Analysis Date = 08/22/16 Pct Recovery = 108% Analysis Date = 08/22/16 Pct Recovery = 108% Analysis Date = 08/17/16 Pct Recovery = 108% Analysis Date = 08/17/16 Pct Recovery = 108% Analysis Date = 08/13/16 Pct Recovery = 108% Analysis Date = 08/13/16 Pct Recovery = 108% Analysis Date = 08/08/16 Pct Recovery = 108% Analysis Date = 08/08/16 Pct Recovery = 108% Analysis Date = 08/03/16 Pct Recovery = 108% Analysis Date = 08/03/16 Pct Recovery = 108% Analysis Date = 07/29/16 Pct Recovery = 108% Analysis Date = 07/29/16 Pct Recovery = 108% Analysis Date = 07/24/16 Pct Recovery = 108% Analysis Date = 07/24/16 Pct Recovery = 108% Analysis Date = 07/20/16 Pct Recovery = 108% Analysis Date = 07/20/16 Pct Recovery = 108% Analysis Date = 07/15/16 Pct Recovery = 108% Analysis Date = 07/15/16 Pct Recovery = 108% Analysis Date = 07/10/16 Pct Recovery = 109% Analysis Date = 07/10/16 Pct Recovery = 109% Analysis Date = 07/05/16 Pct Recovery = 109% Analysis Date = 07/05/16 Pct Recovery = 109% Analysis Date = 06/30/16 Pct Recovery = 109% Analysis Date = 06/30/16 Pct Recovery = 109% Analysis Date = 06/26/16 Pct Recovery = 109% Analysis Date = 06/26/16 Pct Recovery = 109% Analysis Date = 06/21/16 Pct Recovery = 109% Analysis Date = 06/21/16 Pct Recovery = 109% Analysis Date = 06/16/16 Pct Recovery = 109% Analysis Date = 06/16/16 Pct Recovery = 109% Analysis Date = 06/11/16 Pct Recovery = 109% Analysis Date = 06/11/16 Pct Recovery = 109% Analysis Date = 06/06/16 Pct Recovery = 109% Analysis Date = 06/06/16 Pct Recovery = 109% Analysis Date = 06/02/16 Pct Recovery = 109% Analysis Date = 06/02/16 Pct Recovery = 109% Analysis Date = 05/28/16 Pct Recovery = 109% Analysis Date = 05/28/16 Pct Recovery = 109% Analysis Date = 05/23/16 Pct Recovery = 109% Analysis Date = 05/23/16 Pct Recovery = 109% Analysis Date = 05/18/16 Pct Recovery = 109% Analysis Date = 05/18/16 Pct Recovery = 109% Analysis Date = 05/13/16 Pct Recovery = 110% Analysis Date = 05/13/16 Pct Recovery = 110% Analysis Date = 05/09/16 Pct Recovery = 110% Analysis Date = 05/09/16 Pct Recovery = 110% Analysis Date = 05/04/16 Pct Recovery = 110% Analysis Date = 05/04/16 Pct Recovery = 110% Analysis Date = 04/29/16 Pct Recovery = 110% Analysis Date = 04/29/16 Pct Recovery = 110% Analysis Date = 04/24/16 Pct Recovery = 110% Analysis Date = 04/24/16 Pct Recovery = 110% Analysis Date = 04/19/16 Pct Recovery = 110% Analysis Date = 04/19/16 Pct Recovery = 110% Analysis Date = 04/15/16 Pct Recovery = 110% Analysis Date = 04/15/16 Pct Recovery = 110% Analysis Date = 04/10/16 Pct Recovery = 110% Analysis Date = 04/10/16 Pct Recovery = 110% Analysis Date = 04/05/16 Pct Recovery = 110% Analysis Date = 04/05/16 Pct Recovery = 110% Analysis Date = 03/31/16 Pct Recovery = 110% Analysis Date = 03/31/16 Pct Recovery = 110% Analysis Date = 03/26/16 Pct Recovery = 110% Analysis Date = 03/26/16 Pct Recovery = 110% Analysis Date = 03/22/16 Pct Recovery = 110% Analysis Date = 03/22/16 Pct Recovery = 110% Analysis Date = 03/17/16 Pct Recovery = 110% Analysis Date = 03/17/16 Pct Recovery = 110% Analysis Date = 03/12/16 Pct Recovery = 110% Analysis Date = 03/12/16 Pct Recovery = 110% Analysis Date = 03/07/16 Pct Recovery = 110% Analysis Date = 03/07/16 Pct Recovery = 110% Analysis Date = 03/02/16 Pct Recovery = 110% Analysis Date = 03/02/16 Pct Recovery = 110% Analysis Date = 02/27/16 Pct Recovery = 110% Analysis Date = 02/27/16 Pct Recovery = 110% Analysis Date = 02/22/16 Pct Recovery = 110% Analysis Date = 02/22/16 Pct Recovery = 110% Analysis Date = 02/17/16 Pct Recovery = 110% Analysis Date = 02/17/16 Pct Recovery = 110% Analysis Date = 02/12/16 Pct Recovery = 110% Analysis Date = 02/12/16 Pct Recovery = 110% Analysis Date = 02/07/16 Pct Recovery = 110% Analysis Date = 02/07/16 Pct Recovery = 110% Analysis Date = 02/03/16 Pct Recovery = 110% Analysis Date = 02/03/16 Pct Recovery = 110% Analysis Date = 01/29/16 Pct Recovery = 110% Analysis Date = 01/29/16 Pct Recovery = 110% Analysis Date = 01/24/16 Pct Recovery = 110% Analysis Date = 01/24/16 Pct Recovery = 110% Analysis Date = 01/19/16 Pct Recovery = 110% Analysis Date = 01/19/16 Pct Recovery = 110% Analysis Date = 01/14/16 Pct Recovery = 110% Analysis Date = 01/14/16 Pct Recovery = 110% Analysis Date = 01/10/16 Pct Recovery = 110% Analysis Date = 01/10/16 Pct Recovery = 110% Analysis Date = 01/05/16 Pct Recovery = 110% Analysis Date = 01/05/16 Pct Recovery = 110% Analysis Date = 12/31/15 Pct Recovery = 110% Analysis Date = 12/31/15 Pct Recovery = 110% Analysis Date = 12/26/15 Pct Recovery = 110% Analysis Date = 12/26/15 Pct Recovery = 110% Analysis Date = 12/21/15 Pct Recovery = 109% Analysis Date = 12/21/15 Pct Recovery = 109% Analysis Date = 12/17/15 Pct Recovery = 109% Analysis Date = 12/17/15 Pct Recovery = 109% Analysis Date = 12/12/15 Pct Recovery = 109% Analysis Date = 12/12/15 Pct Recovery = 109% Analysis Date = 12/07/15 Pct Recovery = 109% Analysis Date = 12/07/15 Pct Recovery = 109% Analysis Date = 12/02/15 Pct Recovery = 109% Analysis Date = 12/02/15 Pct Recovery = 109% Analysis Date = 11/27/15 Pct Recovery = 108% Analysis Date = 11/27/15 Pct Recovery = 108% Analysis Date = 11/23/15 Pct Recovery = 108% Analysis Date = 11/23/15 Pct Recovery = 108% Analysis Date = 11/18/15 Pct Recovery = 107% Analysis Date = 11/18/15 Pct Recovery = 107% Analysis Date = 11/13/15 Pct Recovery = 107% Analysis Date = 11/13/15 Pct Recovery = 107% Analysis Date = 11/08/15 Pct Recovery = 106% Analysis Date = 11/08/15 Pct Recovery = 106% Analysis Date = 11/03/15 Pct Recovery = 106% Analysis Date = 11/03/15 Pct Recovery = 106% Analysis Date = 10/30/15 Pct Recovery = 105% Analysis Date = 10/30/15 Pct Recovery = 105% Analysis Date = 10/25/15 Pct Recovery = 105% Analysis Date = 10/25/15 Pct Recovery = 105% Analysis Date = 10/20/15 Pct Recovery = 105% Analysis Date = 10/20/15 Pct Recovery = 105% Analysis Date = 10/15/15 Pct Recovery = 104% Analysis Date = 10/15/15 Pct Recovery = 104% Analysis Date = 10/10/15 Pct Recovery = 104% Analysis Date = 10/10/15 Pct Recovery = 104% Analysis Date = 10/06/15 Pct Recovery = 103% Analysis Date = 10/06/15 Pct Recovery = 103% Analysis Date = 10/01/15 Pct Recovery = 102% Analysis Date = 10/01/15 Pct Recovery = 102% Analysis Date = 09/26/15 Pct Recovery = 102% Analysis Date = 09/26/15 Pct Recovery = 102% Analysis Date = 09/21/15 Pct Recovery = 101% Analysis Date = 09/21/15 Pct Recovery = 101% Analysis Date = 09/16/15 Pct Recovery = 101% Analysis Date = 09/16/15 Pct Recovery = 101% Analysis Date = 09/12/15 Pct Recovery = 100% Analysis Date = 09/12/15 Pct Recovery = 100% Analysis Date = 09/07/15 Pct Recovery = 100% Analysis Date = 09/07/15 Pct Recovery = 100% Analysis Date = 09/02/15 Pct Recovery = 99% Analysis Date = 09/02/15 Pct Recovery = 99% Analysis Date = 08/28/15 Pct Recovery = 99% Analysis Date = 08/28/15 Pct Recovery = 99% Analysis Date = 08/23/15 Pct Recovery = 98% Analysis Date = 08/23/15 Pct Recovery = 98% Analysis Date = 08/19/15 Pct Recovery = 98% Analysis Date = 08/19/15 Pct Recovery = 98% Analysis Date = 08/14/15 Pct Recovery = 97% Analysis Date = 08/14/15 Pct Recovery = 97% Analysis Date = 08/09/15 Pct Recovery = 97% Analysis Date = 08/09/15 Pct Recovery = 97% Analysis Date = 08/04/15 Pct Recovery = 96% Analysis Date = 08/04/15 Pct Recovery = 96% Analysis Date = 07/30/15 Pct Recovery = 96% Analysis Date = 07/30/15 Pct Recovery = 96% Analysis Date = 07/26/15 Pct Recovery = 95% Analysis Date = 07/26/15 Pct Recovery = 95% Analysis Date = 07/21/15 Pct Recovery = 94% Analysis Date = 07/21/15 Pct Recovery = 94% Analysis Date = 07/16/15 Pct Recovery = 94% Analysis Date = 07/16/15 Pct Recovery = 94% Analysis Date = 07/11/15 Pct Recovery = 93% Analysis Date = 07/11/15 Pct Recovery = 93% Analysis Date = 07/06/15 Pct Recovery = 93% Analysis Date = 07/06/15 Pct Recovery = 93% Analysis Date = 07/02/15 Pct Recovery = 92% Analysis Date = 07/02/15 Pct Recovery = 92% Analysis Date = 06/27/15 Pct Recovery = 92% Analysis Date = 06/27/15 Pct Recovery = 92% Analysis Date = 06/22/15 Pct Recovery = 91% Analysis Date = 06/22/15 Pct Recovery = 91% Analysis Date = 06/17/15 Pct Recovery = 91% Analysis Date = 06/17/15 Pct Recovery = 91% Analysis Date = 06/12/15 Pct Recovery = 90% Analysis Date = 06/12/15 Pct Recovery = 90% Analysis Date = 06/08/15 Pct Recovery = 90% Analysis Date = 06/08/15 Pct Recovery = 90% Analysis Date = 06/03/15 Pct Recovery = 89% Analysis Date = 06/03/15 Pct Recovery = 89% Analysis Date = 05/29/15 Pct Recovery = 89% Analysis Date = 05/29/15 Pct Recovery = 89% Analysis Date = 05/24/15 Pct Recovery = 88% Analysis Date = 05/24/15 Pct Recovery = 88% Analysis Date = 05/19/15 Pct Recovery = 88% Analysis Date = 05/19/15 Pct Recovery = 88% Analysis Date = 05/15/15 Pct Recovery = 87% Analysis Date = 05/15/15 Pct Recovery = 87% Analysis Date = 05/10/15 Pct Recovery = 87% Analysis Date = 05/10/15 Pct Recovery = 87% Analysis Date = 05/05/15 Pct Recovery = 86% Analysis Date = 05/05/15 Pct Recovery = 86% Analysis Date = 04/30/15 Pct Recovery = 86% Analysis Date = 04/30/15 Pct Recovery = 86% Analysis Date = 04/25/15 Pct Recovery = 86% Analysis Date = 04/25/15 Pct Recovery = 86% Analysis Date = 04/21/15 Pct Recovery = 86% Analysis Date = 04/21/15 Pct Recovery = 86% Analysis Date = 04/16/15 Pct Recovery = 85% Analysis Date = 04/16/15 Pct Recovery = 85% Analysis Date = 04/11/15 Pct Recovery = 85% Analysis Date = 04/11/15 Pct Recovery = 85% Analysis Date = 04/06/15 Pct Recovery = 85% Analysis Date = 04/06/15 Pct Recovery = 85% Analysis Date = 04/01/15 Pct Recovery = 85% Analysis Date = 04/01/15 Pct Recovery = 85% Analysis Date = 03/28/15 Pct Recovery = 85% Analysis Date = 03/28/15 Pct Recovery = 85% Analysis Date = 03/23/15 Pct Recovery = 84% Analysis Date = 03/23/15 Pct Recovery = 84% Analysis Date = 03/18/15 Pct Recovery = 84% Analysis Date = 03/18/15 Pct Recovery = 84% Analysis Date = 03/13/15 Pct Recovery = 84% Analysis Date = 03/13/15 Pct Recovery = 84% Analysis Date = 03/08/15 Pct Recovery = 84% Analysis Date = 03/08/15 Pct Recovery = 84% Analysis Date = 03/04/15 Pct Recovery = 85% Analysis Date = 03/04/15 Pct Recovery = 85% Analysis Date = 02/27/15 Pct Recovery = 85% Analysis Date = 02/27/15 Pct Recovery = 85% Analysis Date = 02/22/15 Pct Recovery = 85% Analysis Date = 02/22/15 Pct Recovery = 85% Analysis Date = 02/17/15 Pct Recovery = 85% Analysis Date = 02/17/15 Pct Recovery = 85% Analysis Date = 02/12/15 Pct Recovery = 85% Analysis Date = 02/12/15 Pct Recovery = 85% Analysis Date = 02/08/15 Pct Recovery = 85% Analysis Date = 02/08/15 Pct Recovery = 85% Analysis Date = 02/03/15 Pct Recovery = 85% Analysis Date = 02/03/15 Pct Recovery = 85% Analysis Date = 01/29/15 Pct Recovery = 85% Analysis Date = 01/29/15 Pct Recovery = 85% Analysis Date = 01/24/15 Pct Recovery = 86% Analysis Date = 01/24/15 Pct Recovery = 86% Analysis Date = 01/19/15 Pct Recovery = 86% Analysis Date = 01/19/15 Pct Recovery = 86% Analysis Date = 01/15/15 Pct Recovery = 86% Analysis Date = 01/15/15 Pct Recovery = 86% Analysis Date = 01/10/15 Pct Recovery = 86% Analysis Date = 01/10/15 Pct Recovery = 86% Analysis Date = 01/05/15 Pct Recovery = 86% Analysis Date = 01/05/15 Pct Recovery = 86% Analysis Date = 12/31/14 Pct Recovery = 86% Analysis Date = 12/31/14 Pct Recovery = 86% Analysis Date = 12/26/14 Pct Recovery = 86% Analysis Date = 12/26/14 Pct Recovery = 86% Analysis Date = 12/22/14 Pct Recovery = 86% Analysis Date = 12/22/14 Pct Recovery = 86% Analysis Date = 12/17/14 Pct Recovery = 87% Analysis Date = 12/17/14 Pct Recovery = 87% Analysis Date = 12/12/14 Pct Recovery = 87% Analysis Date = 12/12/14 Pct Recovery = 87% Analysis Date = 12/07/14 Pct Recovery = 87% Analysis Date = 12/07/14 Pct Recovery = 87% Analysis Date = 12/02/14 Pct Recovery = 87% Analysis Date = 12/02/14 Pct Recovery = 87% Analysis Date = 11/28/14 Pct Recovery = 87% Analysis Date = 11/28/14 Pct Recovery = 87% Analysis Date = 11/23/14 Pct Recovery = 87% Analysis Date = 11/23/14 Pct Recovery = 87% Analysis Date = 11/18/14 Pct Recovery = 87% Analysis Date = 11/18/14 Pct Recovery = 87% Analysis Date = 11/13/14 Pct Recovery = 88% Analysis Date = 11/13/14 Pct Recovery = 88% Analysis Date = 11/08/14 Pct Recovery = 88% Analysis Date = 11/08/14 Pct Recovery = 88% Analysis Date = 11/04/14 Pct Recovery = 88% Analysis Date = 11/04/14 Pct Recovery = 88% Analysis Date = 10/30/14 Pct Recovery = 88% Analysis Date = 10/30/14 Pct Recovery = 88% Analysis Date = 10/25/14 Pct Recovery = 88% Analysis Date = 10/25/14 Pct Recovery = 88% Analysis Date = 10/20/14 Pct Recovery = 89% Analysis Date = 10/20/14 Pct Recovery = 89% Analysis Date = 10/15/14 Pct Recovery = 89% Analysis Date = 10/15/14 Pct Recovery = 89% Analysis Date = 10/11/14 Pct Recovery = 89% Analysis Date = 10/11/14 Pct Recovery = 89% Analysis Date = 10/06/14 Pct Recovery = 89% Analysis Date = 10/06/14 Pct Recovery = 89% Analysis Date = 10/01/14 Pct Recovery = 89% Analysis Date = 10/01/14 Pct Recovery = 89% Analysis Date = 09/26/14 Pct Recovery = 90% Analysis Date = 09/26/14 Pct Recovery = 90% Analysis Date = 09/21/14 Pct Recovery = 90% Analysis Date = 09/21/14 Pct Recovery = 90% Analysis Date = 09/17/14 Pct Recovery = 90% Analysis Date = 09/17/14 Pct Recovery = 90% Analysis Date = 09/12/14 Pct Recovery = 90% Analysis Date = 09/12/14 Pct Recovery = 90% Analysis Date = 09/07/14 Pct Recovery = 91% Analysis Date = 09/07/14 Pct Recovery = 91% Analysis Date = 09/02/14 Pct Recovery = 91% Analysis Date = 09/02/14 Pct Recovery = 91% Analysis Date = 08/28/14 Pct Recovery = 91% Analysis Date = 08/28/14 Pct Recovery = 91% Analysis Date = 08/24/14 Pct Recovery = 91% Analysis Date = 08/24/14 Pct Recovery = 91% Analysis Date = 08/19/14 Pct Recovery = 92% Analysis Date = 08/19/14 Pct Recovery = 92% Analysis Date = 08/14/14 Pct Recovery = 92% Analysis Date = 08/14/14 Pct Recovery = 92% Analysis Date = 08/09/14 Pct Recovery = 92% Analysis Date = 08/09/14 Pct Recovery = 92% Analysis Date = 08/04/14 Pct Recovery = 93% Analysis Date = 08/04/14 Pct Recovery = 93% Analysis Date = 07/31/14 Pct Recovery = 93% Analysis Date = 07/31/14 Pct Recovery = 93% Analysis Date = 07/26/14 Pct Recovery = 93% Analysis Date = 07/26/14 Pct Recovery = 93% Analysis Date = 07/21/14 Pct Recovery = 93% Analysis Date = 07/21/14 Pct Recovery = 93% Analysis Date = 07/16/14 Pct Recovery = 94% Analysis Date = 07/16/14 Pct Recovery = 94% Analysis Date = 07/11/14 Pct Recovery = 94% Analysis Date = 07/11/14 Pct Recovery = 94% Analysis Date = 07/07/14 Pct Recovery = 94% Analysis Date = 07/07/14 Pct Recovery = 94% Analysis Date = 07/02/14 Pct Recovery = 95% Analysis Date = 07/02/14 Pct Recovery = 95% Analysis Date = 06/27/14 Pct Recovery = 95% Analysis Date = 06/27/14 Pct Recovery = 95% Analysis Date = 06/22/14 Pct Recovery = 95% Analysis Date = 06/22/14 Pct Recovery = 95% Analysis Date = 06/17/14 Pct Recovery = 96% Analysis Date = 06/17/14 Pct Recovery = 96% Analysis Date = 06/13/14 Pct Recovery = 96% Analysis Date = 06/13/14 Pct Recovery = 96% Analysis Date = 06/08/14 Pct Recovery = 96% Analysis Date = 06/08/14 Pct Recovery = 96% Analysis Date = 06/03/14 Pct Recovery = 97% Analysis Date = 06/03/14 Pct Recovery = 97% Analysis Date = 05/29/14 Pct Recovery = 97% Analysis Date = 05/29/14 Pct Recovery = 97% Analysis Date = 05/24/14 Pct Recovery = 97% Analysis Date = 05/24/14 Pct Recovery = 97% Analysis Date = 05/20/14 Pct Recovery = 98% Analysis Date = 05/20/14 Pct Recovery = 98% Analysis Date = 05/15/14 Pct Recovery = 98% Analysis Date = 05/15/14 Pct Recovery = 98% Analysis Date = 05/10/14 Pct Recovery = 98% Analysis Date = 05/10/14 Pct Recovery = 98% Analysis Date = 05/05/14 Pct Recovery = 99% Analysis Date = 05/05/14 Pct Recovery = 99% Analysis Date = 05/01/14 Pct Recovery = 99% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
N-PENTANE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 2 112% 12% 112% 12%
>= Reporting Level 46 99% 27% 103% 24%
Total 48 100% 26% 104% 23%

Sample Statistics
N-PENTANE

Characteristic N % % Basis
Plotted 48 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 48 .  
False Negatives 0 0% 0 out of 48
Not Spiked 25 .  
False Positives 0 0% 0 out of 25

BQS OBSP Determination:
N-PROPYLBENZENE
METHOD: 4440 , TESTIDCODE: 77224GCM66
Open Data Set

Analysis Date = 12/16/16 SpikeMix = NSI 041816AVOC: 40 µl & ChemService 5082900: 40 µl Pct Recovery = 78% Analysis Date = 12/12/16 SpikeMix = Accu 216041125: 40 µl & Crescent 03FF058: 40 µl Pct Recovery = 120% Analysis Date = 08/04/16 SpikeMix = Crescent 03FF058: 40 µl & Supelco LC20141V: 40 µl Pct Recovery = 81% Analysis Date = 07/14/16 SpikeMix = Accu 216041125: 40 µl & NSI 041816AVOC: 40 µl Pct Recovery = 105% Analysis Date = 11/21/16 SpikeMix = Crescent 03FF058: 25 µl & Supelco LC20141V: 25 µl Pct Recovery = 85% Analysis Date = 08/26/16 SpikeMix = NSI 041816AVOC: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 79% Analysis Date = 06/30/16 SpikeMix = Crescent 03FF058: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 85% Analysis Date = 06/21/16 SpikeMix = Phenova B20160319: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 109% Analysis Date = 05/24/16 SpikeMix = Accu 216041125: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 109% Analysis Date = 03/06/15 SpikeMix = ERA 0227-14-06.1A: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 84% Analysis Date = 12/17/14 SpikeMix = Supelco LC06438: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 93% Analysis Date = 09/21/14 SpikeMix = Supelco LC06438: 20 µl Pct Recovery = 88% Analysis Date = 06/10/14 SpikeMix = NSI 032614: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 107% Analysis Date = 03/19/15 SpikeMix = Spex Organics C1140417015: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 103% Analysis Date = 11/22/14 SpikeMix = NSI 032614: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 91% Analysis Date = 08/19/14 SpikeMix = Spex Organics C1140417015: 20 µl & Accu 214031115: 20 µl Pct Recovery = 94% Analysis Date = 08/16/14 SpikeMix = ERA 0227-14-06.1A: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 90% Analysis Date = 09/29/15 SpikeMix = Accu 215041380: 25 µl & ERA 0406-15-03: 25 µl Pct Recovery = 106% Analysis Date = 06/16/15 SpikeMix = ERA 0406-15-03: 25 µl & Supelco LC13545: 25 µl Pct Recovery = 76% Analysis Date = 07/13/15 SpikeMix = Crescent 04EE008: 25 µl & NSI 050515AVOC: 25 µl Pct Recovery = 96% Analysis Date = 10/13/16 SpikeMix = Accu 216041125: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 108% Analysis Date = 10/13/16 SpikeMix = NSI 041816AVOC: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 77% Analysis Date = 09/28/16 SpikeMix = Crescent 03FF058: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 74% Analysis Date = 09/08/16 SpikeMix = Phenova B20160319: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 90% Analysis Date = 08/20/16 SpikeMix = Accu 216041125: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 100% Analysis Date = 07/29/16 SpikeMix = Phenova B20160319: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 106% Analysis Date = 06/10/16 SpikeMix = NSI 041816AVOC: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 87% Analysis Date = 04/26/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 82% Analysis Date = 03/04/16 SpikeMix = Accu 215041380: 15 µl & ERA 0406-15-03: 15 µl Pct Recovery = 94% Analysis Date = 02/05/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 88% Analysis Date = 10/16/15 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 82% Analysis Date = 11/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 88% Analysis Date = 10/17/15 SpikeMix = Crescent 04EE008: 15 µl & NSI 050515AVOC: 15 µl Pct Recovery = 105% Analysis Date = 06/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Accu 215041380: 15 µl Pct Recovery = 105% Analysis Date = 10/21/14 SpikeMix = ERA 0227-14-06.1A: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 92% Analysis Date = 06/18/14 SpikeMix = Supelco LC06438: 10 µl & Accu 214031115: 10 µl Pct Recovery = 87% Analysis Date = 05/30/14 SpikeMix = NSI 032614: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 75% Analysis Date = 05/03/14 SpikeMix = Crescent 03DD004: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 105% Analysis Date = 11/06/14 SpikeMix = Spex Organics C1140417015: 10 µl & Crescent 03DD004: 10 µl Pct Recovery = 112% Analysis Date = 09/09/14 SpikeMix = NSI 032614: 10 µl & Spex Organics C1140417015: 10 µl Pct Recovery = 128% Analysis Date = 07/23/14 SpikeMix = Spex Organics C1140417015: 10 µl & Accu 214031115: 10 µl Pct Recovery = 108% Analysis Date = 07/11/14 SpikeMix = Spex Organics C1140417015: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 93% Analysis Date = 11/20/15 SpikeMix = Accu 215041380: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 105% Analysis Date = 07/31/15 SpikeMix = Crescent 04EE008: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 86% Analysis Date = 06/27/15 SpikeMix = ERA 0406-15-03: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 111% Analysis Date = 03/17/16 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 89% Analysis Date = 01/27/16 SpikeMix = Crescent 04EE008: 10 µl & NSI 050515AVOC: 10 µl Pct Recovery = 102% Analysis Date = 12/10/15 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 98% Analysis Date = 09/03/15 SpikeMix = NSI 050515AVOC: 10 µl & Spex Organics EN150428007: 10 µl Pct Recovery = 87% Analysis Date = 12/16/16 Pct Recovery = 91% Analysis Date = 12/11/16 Pct Recovery = 91% Analysis Date = 12/11/16 Pct Recovery = 91% Analysis Date = 12/06/16 Pct Recovery = 91% Analysis Date = 12/06/16 Pct Recovery = 91% Analysis Date = 12/01/16 Pct Recovery = 91% Analysis Date = 12/01/16 Pct Recovery = 91% Analysis Date = 11/26/16 Pct Recovery = 91% Analysis Date = 11/26/16 Pct Recovery = 91% Analysis Date = 11/22/16 Pct Recovery = 91% Analysis Date = 11/22/16 Pct Recovery = 91% Analysis Date = 11/17/16 Pct Recovery = 91% Analysis Date = 11/17/16 Pct Recovery = 91% Analysis Date = 11/12/16 Pct Recovery = 92% Analysis Date = 11/12/16 Pct Recovery = 92% Analysis Date = 11/07/16 Pct Recovery = 92% Analysis Date = 11/07/16 Pct Recovery = 92% Analysis Date = 11/02/16 Pct Recovery = 92% Analysis Date = 11/02/16 Pct Recovery = 92% Analysis Date = 10/29/16 Pct Recovery = 92% Analysis Date = 10/29/16 Pct Recovery = 92% Analysis Date = 10/24/16 Pct Recovery = 92% Analysis Date = 10/24/16 Pct Recovery = 92% Analysis Date = 10/19/16 Pct Recovery = 92% Analysis Date = 10/19/16 Pct Recovery = 92% Analysis Date = 10/14/16 Pct Recovery = 92% Analysis Date = 10/14/16 Pct Recovery = 92% Analysis Date = 10/09/16 Pct Recovery = 92% Analysis Date = 10/09/16 Pct Recovery = 92% Analysis Date = 10/05/16 Pct Recovery = 92% Analysis Date = 10/05/16 Pct Recovery = 92% Analysis Date = 09/30/16 Pct Recovery = 92% Analysis Date = 09/30/16 Pct Recovery = 92% Analysis Date = 09/25/16 Pct Recovery = 92% Analysis Date = 09/25/16 Pct Recovery = 92% Analysis Date = 09/20/16 Pct Recovery = 92% Analysis Date = 09/20/16 Pct Recovery = 92% Analysis Date = 09/15/16 Pct Recovery = 92% Analysis Date = 09/15/16 Pct Recovery = 92% Analysis Date = 09/11/16 Pct Recovery = 92% Analysis Date = 09/11/16 Pct Recovery = 92% Analysis Date = 09/06/16 Pct Recovery = 92% Analysis Date = 09/06/16 Pct Recovery = 92% Analysis Date = 09/01/16 Pct Recovery = 92% Analysis Date = 09/01/16 Pct Recovery = 92% Analysis Date = 08/27/16 Pct Recovery = 92% Analysis Date = 08/27/16 Pct Recovery = 92% Analysis Date = 08/23/16 Pct Recovery = 92% Analysis Date = 08/23/16 Pct Recovery = 92% Analysis Date = 08/18/16 Pct Recovery = 92% Analysis Date = 08/18/16 Pct Recovery = 92% Analysis Date = 08/13/16 Pct Recovery = 93% Analysis Date = 08/13/16 Pct Recovery = 93% Analysis Date = 08/08/16 Pct Recovery = 93% Analysis Date = 08/08/16 Pct Recovery = 93% Analysis Date = 08/03/16 Pct Recovery = 93% Analysis Date = 08/03/16 Pct Recovery = 93% Analysis Date = 07/30/16 Pct Recovery = 93% Analysis Date = 07/30/16 Pct Recovery = 93% Analysis Date = 07/25/16 Pct Recovery = 93% Analysis Date = 07/25/16 Pct Recovery = 93% Analysis Date = 07/20/16 Pct Recovery = 93% Analysis Date = 07/20/16 Pct Recovery = 93% Analysis Date = 07/15/16 Pct Recovery = 93% Analysis Date = 07/15/16 Pct Recovery = 93% Analysis Date = 07/10/16 Pct Recovery = 93% Analysis Date = 07/10/16 Pct Recovery = 93% Analysis Date = 07/06/16 Pct Recovery = 93% Analysis Date = 07/06/16 Pct Recovery = 93% Analysis Date = 07/01/16 Pct Recovery = 93% Analysis Date = 07/01/16 Pct Recovery = 93% Analysis Date = 06/26/16 Pct Recovery = 93% Analysis Date = 06/26/16 Pct Recovery = 93% Analysis Date = 06/21/16 Pct Recovery = 93% Analysis Date = 06/21/16 Pct Recovery = 93% Analysis Date = 06/16/16 Pct Recovery = 93% Analysis Date = 06/16/16 Pct Recovery = 93% Analysis Date = 06/12/16 Pct Recovery = 93% Analysis Date = 06/12/16 Pct Recovery = 93% Analysis Date = 06/07/16 Pct Recovery = 93% Analysis Date = 06/07/16 Pct Recovery = 93% Analysis Date = 06/02/16 Pct Recovery = 93% Analysis Date = 06/02/16 Pct Recovery = 93% Analysis Date = 05/28/16 Pct Recovery = 93% Analysis Date = 05/28/16 Pct Recovery = 93% Analysis Date = 05/24/16 Pct Recovery = 93% Analysis Date = 05/24/16 Pct Recovery = 93% Analysis Date = 05/19/16 Pct Recovery = 94% Analysis Date = 05/19/16 Pct Recovery = 94% Analysis Date = 05/14/16 Pct Recovery = 94% Analysis Date = 05/14/16 Pct Recovery = 94% Analysis Date = 05/09/16 Pct Recovery = 94% Analysis Date = 05/09/16 Pct Recovery = 94% Analysis Date = 05/04/16 Pct Recovery = 94% Analysis Date = 05/04/16 Pct Recovery = 94% Analysis Date = 04/30/16 Pct Recovery = 94% Analysis Date = 04/30/16 Pct Recovery = 94% Analysis Date = 04/25/16 Pct Recovery = 94% Analysis Date = 04/25/16 Pct Recovery = 94% Analysis Date = 04/20/16 Pct Recovery = 94% Analysis Date = 04/20/16 Pct Recovery = 94% Analysis Date = 04/15/16 Pct Recovery = 94% Analysis Date = 04/15/16 Pct Recovery = 94% Analysis Date = 04/10/16 Pct Recovery = 94% Analysis Date = 04/10/16 Pct Recovery = 94% Analysis Date = 04/06/16 Pct Recovery = 94% Analysis Date = 04/06/16 Pct Recovery = 94% Analysis Date = 04/01/16 Pct Recovery = 94% Analysis Date = 04/01/16 Pct Recovery = 94% Analysis Date = 03/27/16 Pct Recovery = 94% Analysis Date = 03/27/16 Pct Recovery = 94% Analysis Date = 03/22/16 Pct Recovery = 94% Analysis Date = 03/22/16 Pct Recovery = 94% Analysis Date = 03/17/16 Pct Recovery = 95% Analysis Date = 03/17/16 Pct Recovery = 95% Analysis Date = 03/13/16 Pct Recovery = 95% Analysis Date = 03/13/16 Pct Recovery = 95% Analysis Date = 03/08/16 Pct Recovery = 95% Analysis Date = 03/08/16 Pct Recovery = 95% Analysis Date = 03/03/16 Pct Recovery = 95% Analysis Date = 03/03/16 Pct Recovery = 95% Analysis Date = 02/27/16 Pct Recovery = 95% Analysis Date = 02/27/16 Pct Recovery = 95% Analysis Date = 02/23/16 Pct Recovery = 95% Analysis Date = 02/23/16 Pct Recovery = 95% Analysis Date = 02/18/16 Pct Recovery = 95% Analysis Date = 02/18/16 Pct Recovery = 95% Analysis Date = 02/13/16 Pct Recovery = 95% Analysis Date = 02/13/16 Pct Recovery = 95% Analysis Date = 02/08/16 Pct Recovery = 95% Analysis Date = 02/08/16 Pct Recovery = 95% Analysis Date = 02/03/16 Pct Recovery = 95% Analysis Date = 02/03/16 Pct Recovery = 95% Analysis Date = 01/30/16 Pct Recovery = 95% Analysis Date = 01/30/16 Pct Recovery = 95% Analysis Date = 01/25/16 Pct Recovery = 95% Analysis Date = 01/25/16 Pct Recovery = 95% Analysis Date = 01/20/16 Pct Recovery = 95% Analysis Date = 01/20/16 Pct Recovery = 95% Analysis Date = 01/15/16 Pct Recovery = 95% Analysis Date = 01/15/16 Pct Recovery = 95% Analysis Date = 01/10/16 Pct Recovery = 95% Analysis Date = 01/10/16 Pct Recovery = 95% Analysis Date = 01/06/16 Pct Recovery = 95% Analysis Date = 01/06/16 Pct Recovery = 95% Analysis Date = 01/01/16 Pct Recovery = 95% Analysis Date = 01/01/16 Pct Recovery = 95% Analysis Date = 12/27/15 Pct Recovery = 95% Analysis Date = 12/27/15 Pct Recovery = 95% Analysis Date = 12/22/15 Pct Recovery = 95% Analysis Date = 12/22/15 Pct Recovery = 95% Analysis Date = 12/17/15 Pct Recovery = 95% Analysis Date = 12/17/15 Pct Recovery = 95% Analysis Date = 12/13/15 Pct Recovery = 95% Analysis Date = 12/13/15 Pct Recovery = 95% Analysis Date = 12/08/15 Pct Recovery = 95% Analysis Date = 12/08/15 Pct Recovery = 95% Analysis Date = 12/03/15 Pct Recovery = 95% Analysis Date = 12/03/15 Pct Recovery = 95% Analysis Date = 11/28/15 Pct Recovery = 95% Analysis Date = 11/28/15 Pct Recovery = 95% Analysis Date = 11/24/15 Pct Recovery = 95% Analysis Date = 11/24/15 Pct Recovery = 95% Analysis Date = 11/19/15 Pct Recovery = 95% Analysis Date = 11/19/15 Pct Recovery = 95% Analysis Date = 11/14/15 Pct Recovery = 95% Analysis Date = 11/14/15 Pct Recovery = 95% Analysis Date = 11/09/15 Pct Recovery = 95% Analysis Date = 11/09/15 Pct Recovery = 95% Analysis Date = 11/04/15 Pct Recovery = 95% Analysis Date = 11/04/15 Pct Recovery = 95% Analysis Date = 10/31/15 Pct Recovery = 95% Analysis Date = 10/31/15 Pct Recovery = 95% Analysis Date = 10/26/15 Pct Recovery = 95% Analysis Date = 10/26/15 Pct Recovery = 95% Analysis Date = 10/21/15 Pct Recovery = 95% Analysis Date = 10/21/15 Pct Recovery = 95% Analysis Date = 10/16/15 Pct Recovery = 95% Analysis Date = 10/16/15 Pct Recovery = 95% Analysis Date = 10/11/15 Pct Recovery = 95% Analysis Date = 10/11/15 Pct Recovery = 95% Analysis Date = 10/07/15 Pct Recovery = 95% Analysis Date = 10/07/15 Pct Recovery = 95% Analysis Date = 10/02/15 Pct Recovery = 95% Analysis Date = 10/02/15 Pct Recovery = 95% Analysis Date = 09/27/15 Pct Recovery = 95% Analysis Date = 09/27/15 Pct Recovery = 95% Analysis Date = 09/22/15 Pct Recovery = 95% Analysis Date = 09/22/15 Pct Recovery = 95% Analysis Date = 09/17/15 Pct Recovery = 95% Analysis Date = 09/17/15 Pct Recovery = 95% Analysis Date = 09/13/15 Pct Recovery = 95% Analysis Date = 09/13/15 Pct Recovery = 95% Analysis Date = 09/08/15 Pct Recovery = 95% Analysis Date = 09/08/15 Pct Recovery = 95% Analysis Date = 09/03/15 Pct Recovery = 95% Analysis Date = 09/03/15 Pct Recovery = 95% Analysis Date = 08/29/15 Pct Recovery = 95% Analysis Date = 08/29/15 Pct Recovery = 95% Analysis Date = 08/25/15 Pct Recovery = 95% Analysis Date = 08/25/15 Pct Recovery = 95% Analysis Date = 08/20/15 Pct Recovery = 95% Analysis Date = 08/20/15 Pct Recovery = 95% Analysis Date = 08/15/15 Pct Recovery = 95% Analysis Date = 08/15/15 Pct Recovery = 95% Analysis Date = 08/10/15 Pct Recovery = 95% Analysis Date = 08/10/15 Pct Recovery = 95% Analysis Date = 08/05/15 Pct Recovery = 95% Analysis Date = 08/05/15 Pct Recovery = 95% Analysis Date = 08/01/15 Pct Recovery = 95% Analysis Date = 08/01/15 Pct Recovery = 95% Analysis Date = 07/27/15 Pct Recovery = 95% Analysis Date = 07/27/15 Pct Recovery = 95% Analysis Date = 07/22/15 Pct Recovery = 95% Analysis Date = 07/22/15 Pct Recovery = 95% Analysis Date = 07/17/15 Pct Recovery = 95% Analysis Date = 07/17/15 Pct Recovery = 95% Analysis Date = 07/12/15 Pct Recovery = 95% Analysis Date = 07/12/15 Pct Recovery = 95% Analysis Date = 07/08/15 Pct Recovery = 95% Analysis Date = 07/08/15 Pct Recovery = 95% Analysis Date = 07/03/15 Pct Recovery = 95% Analysis Date = 07/03/15 Pct Recovery = 95% Analysis Date = 06/28/15 Pct Recovery = 95% Analysis Date = 06/28/15 Pct Recovery = 95% Analysis Date = 06/23/15 Pct Recovery = 95% Analysis Date = 06/23/15 Pct Recovery = 95% Analysis Date = 06/18/15 Pct Recovery = 95% Analysis Date = 06/18/15 Pct Recovery = 95% Analysis Date = 06/14/15 Pct Recovery = 95% Analysis Date = 06/14/15 Pct Recovery = 95% Analysis Date = 06/09/15 Pct Recovery = 95% Analysis Date = 06/09/15 Pct Recovery = 95% Analysis Date = 06/04/15 Pct Recovery = 95% Analysis Date = 06/04/15 Pct Recovery = 95% Analysis Date = 05/30/15 Pct Recovery = 95% Analysis Date = 05/30/15 Pct Recovery = 95% Analysis Date = 05/25/15 Pct Recovery = 96% Analysis Date = 05/25/15 Pct Recovery = 96% Analysis Date = 05/21/15 Pct Recovery = 96% Analysis Date = 05/21/15 Pct Recovery = 96% Analysis Date = 05/16/15 Pct Recovery = 96% Analysis Date = 05/16/15 Pct Recovery = 96% Analysis Date = 05/11/15 Pct Recovery = 96% Analysis Date = 05/11/15 Pct Recovery = 96% Analysis Date = 05/06/15 Pct Recovery = 96% Analysis Date = 05/06/15 Pct Recovery = 96% Analysis Date = 05/02/15 Pct Recovery = 96% Analysis Date = 05/02/15 Pct Recovery = 96% Analysis Date = 04/27/15 Pct Recovery = 96% Analysis Date = 04/27/15 Pct Recovery = 96% Analysis Date = 04/22/15 Pct Recovery = 96% Analysis Date = 04/22/15 Pct Recovery = 96% Analysis Date = 04/17/15 Pct Recovery = 96% Analysis Date = 04/17/15 Pct Recovery = 96% Analysis Date = 04/12/15 Pct Recovery = 96% Analysis Date = 04/12/15 Pct Recovery = 96% Analysis Date = 04/08/15 Pct Recovery = 96% Analysis Date = 04/08/15 Pct Recovery = 96% Analysis Date = 04/03/15 Pct Recovery = 96% Analysis Date = 04/03/15 Pct Recovery = 96% Analysis Date = 03/29/15 Pct Recovery = 96% Analysis Date = 03/29/15 Pct Recovery = 96% Analysis Date = 03/24/15 Pct Recovery = 96% Analysis Date = 03/24/15 Pct Recovery = 96% Analysis Date = 03/19/15 Pct Recovery = 96% Analysis Date = 03/19/15 Pct Recovery = 96% Analysis Date = 03/15/15 Pct Recovery = 96% Analysis Date = 03/15/15 Pct Recovery = 96% Analysis Date = 03/10/15 Pct Recovery = 96% Analysis Date = 03/10/15 Pct Recovery = 96% Analysis Date = 03/05/15 Pct Recovery = 96% Analysis Date = 03/05/15 Pct Recovery = 96% Analysis Date = 02/28/15 Pct Recovery = 96% Analysis Date = 02/28/15 Pct Recovery = 96% Analysis Date = 02/23/15 Pct Recovery = 96% Analysis Date = 02/23/15 Pct Recovery = 96% Analysis Date = 02/19/15 Pct Recovery = 96% Analysis Date = 02/19/15 Pct Recovery = 96% Analysis Date = 02/14/15 Pct Recovery = 96% Analysis Date = 02/14/15 Pct Recovery = 96% Analysis Date = 02/09/15 Pct Recovery = 96% Analysis Date = 02/09/15 Pct Recovery = 96% Analysis Date = 02/04/15 Pct Recovery = 96% Analysis Date = 02/04/15 Pct Recovery = 96% Analysis Date = 01/31/15 Pct Recovery = 96% Analysis Date = 01/31/15 Pct Recovery = 96% Analysis Date = 01/26/15 Pct Recovery = 96% Analysis Date = 01/26/15 Pct Recovery = 96% Analysis Date = 01/21/15 Pct Recovery = 96% Analysis Date = 01/21/15 Pct Recovery = 96% Analysis Date = 01/16/15 Pct Recovery = 96% Analysis Date = 01/16/15 Pct Recovery = 96% Analysis Date = 01/11/15 Pct Recovery = 96% Analysis Date = 01/11/15 Pct Recovery = 96% Analysis Date = 01/07/15 Pct Recovery = 96% Analysis Date = 01/07/15 Pct Recovery = 96% Analysis Date = 01/02/15 Pct Recovery = 96% Analysis Date = 01/02/15 Pct Recovery = 96% Analysis Date = 12/28/14 Pct Recovery = 96% Analysis Date = 12/28/14 Pct Recovery = 96% Analysis Date = 12/23/14 Pct Recovery = 96% Analysis Date = 12/23/14 Pct Recovery = 96% Analysis Date = 12/18/14 Pct Recovery = 96% Analysis Date = 12/18/14 Pct Recovery = 96% Analysis Date = 12/14/14 Pct Recovery = 96% Analysis Date = 12/14/14 Pct Recovery = 96% Analysis Date = 12/09/14 Pct Recovery = 96% Analysis Date = 12/09/14 Pct Recovery = 96% Analysis Date = 12/04/14 Pct Recovery = 97% Analysis Date = 12/04/14 Pct Recovery = 97% Analysis Date = 11/29/14 Pct Recovery = 97% Analysis Date = 11/29/14 Pct Recovery = 97% Analysis Date = 11/24/14 Pct Recovery = 97% Analysis Date = 11/24/14 Pct Recovery = 97% Analysis Date = 11/20/14 Pct Recovery = 97% Analysis Date = 11/20/14 Pct Recovery = 97% Analysis Date = 11/15/14 Pct Recovery = 97% Analysis Date = 11/15/14 Pct Recovery = 97% Analysis Date = 11/10/14 Pct Recovery = 97% Analysis Date = 11/10/14 Pct Recovery = 97% Analysis Date = 11/05/14 Pct Recovery = 97% Analysis Date = 11/05/14 Pct Recovery = 97% Analysis Date = 11/01/14 Pct Recovery = 97% Analysis Date = 11/01/14 Pct Recovery = 97% Analysis Date = 10/27/14 Pct Recovery = 97% Analysis Date = 10/27/14 Pct Recovery = 97% Analysis Date = 10/22/14 Pct Recovery = 97% Analysis Date = 10/22/14 Pct Recovery = 97% Analysis Date = 10/17/14 Pct Recovery = 97% Analysis Date = 10/17/14 Pct Recovery = 97% Analysis Date = 10/12/14 Pct Recovery = 97% Analysis Date = 10/12/14 Pct Recovery = 97% Analysis Date = 10/08/14 Pct Recovery = 97% Analysis Date = 10/08/14 Pct Recovery = 97% Analysis Date = 10/03/14 Pct Recovery = 97% Analysis Date = 10/03/14 Pct Recovery = 97% Analysis Date = 09/28/14 Pct Recovery = 97% Analysis Date = 09/28/14 Pct Recovery = 97% Analysis Date = 09/23/14 Pct Recovery = 97% Analysis Date = 09/23/14 Pct Recovery = 97% Analysis Date = 09/18/14 Pct Recovery = 97% Analysis Date = 09/18/14 Pct Recovery = 97% Analysis Date = 09/14/14 Pct Recovery = 97% Analysis Date = 09/14/14 Pct Recovery = 97% Analysis Date = 09/09/14 Pct Recovery = 97% Analysis Date = 09/09/14 Pct Recovery = 97% Analysis Date = 09/04/14 Pct Recovery = 97% Analysis Date = 09/04/14 Pct Recovery = 97% Analysis Date = 08/30/14 Pct Recovery = 97% Analysis Date = 08/30/14 Pct Recovery = 97% Analysis Date = 08/25/14 Pct Recovery = 97% Analysis Date = 08/25/14 Pct Recovery = 97% Analysis Date = 08/21/14 Pct Recovery = 97% Analysis Date = 08/21/14 Pct Recovery = 97% Analysis Date = 08/16/14 Pct Recovery = 97% Analysis Date = 08/16/14 Pct Recovery = 97% Analysis Date = 08/11/14 Pct Recovery = 97% Analysis Date = 08/11/14 Pct Recovery = 97% Analysis Date = 08/06/14 Pct Recovery = 97% Analysis Date = 08/06/14 Pct Recovery = 97% Analysis Date = 08/02/14 Pct Recovery = 97% Analysis Date = 08/02/14 Pct Recovery = 97% Analysis Date = 07/28/14 Pct Recovery = 97% Analysis Date = 07/28/14 Pct Recovery = 97% Analysis Date = 07/23/14 Pct Recovery = 97% Analysis Date = 07/23/14 Pct Recovery = 97% Analysis Date = 07/18/14 Pct Recovery = 97% Analysis Date = 07/18/14 Pct Recovery = 97% Analysis Date = 07/13/14 Pct Recovery = 97% Analysis Date = 07/13/14 Pct Recovery = 97% Analysis Date = 07/09/14 Pct Recovery = 97% Analysis Date = 07/09/14 Pct Recovery = 97% Analysis Date = 07/04/14 Pct Recovery = 97% Analysis Date = 07/04/14 Pct Recovery = 97% Analysis Date = 06/29/14 Pct Recovery = 97% Analysis Date = 06/29/14 Pct Recovery = 97% Analysis Date = 06/24/14 Pct Recovery = 97% Analysis Date = 06/24/14 Pct Recovery = 97% Analysis Date = 06/19/14 Pct Recovery = 97% Analysis Date = 06/19/14 Pct Recovery = 97% Analysis Date = 06/15/14 Pct Recovery = 97% Analysis Date = 06/15/14 Pct Recovery = 97% Analysis Date = 06/10/14 Pct Recovery = 97% Analysis Date = 06/10/14 Pct Recovery = 97% Analysis Date = 06/05/14 Pct Recovery = 97% Analysis Date = 06/05/14 Pct Recovery = 97% Analysis Date = 05/31/14 Pct Recovery = 97% Analysis Date = 05/31/14 Pct Recovery = 97% Analysis Date = 05/26/14 Pct Recovery = 97% Analysis Date = 05/26/14 Pct Recovery = 97% Analysis Date = 05/22/14 Pct Recovery = 97% Analysis Date = 05/22/14 Pct Recovery = 97% Analysis Date = 05/17/14 Pct Recovery = 97% Analysis Date = 05/17/14 Pct Recovery = 97% Analysis Date = 05/12/14 Pct Recovery = 97% Analysis Date = 05/12/14 Pct Recovery = 97% Analysis Date = 05/07/14 Pct Recovery = 97% Analysis Date = 05/07/14 Pct Recovery = 97% Analysis Date = 05/03/14 Pct Recovery = 97% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
N-PROPYLBENZENE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 49 95% 13% 93% 14%
Total 49 95% 13% 93% 14%

Sample Statistics
N-PROPYLBENZENE

Characteristic N % % Basis
Plotted 49 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 49 .  
False Negatives 0 0% 0 out of 49
Not Spiked 24 .  
False Positives 0 0% 0 out of 24

BQS OBSP Determination:
NAPHTHALENE
METHOD: 4440 , TESTIDCODE: 34696GCM66
Open Data Set

Analysis Date = 12/16/16 SpikeMix = NSI 041816AVOC: 40 µl & ChemService 5082900: 40 µl Pct Recovery = 88% Analysis Date = 08/04/16 SpikeMix = Crescent 03FF058: 40 µl & Supelco LC20141V: 40 µl Pct Recovery = 70% Analysis Date = 07/20/16 SpikeMix = Supelco LC20141V: 40 µl & Accu 216041125: 40 µl Pct Recovery = 84% Analysis Date = 11/21/16 SpikeMix = Crescent 03FF058: 25 µl & Supelco LC20141V: 25 µl Pct Recovery = 87% Analysis Date = 09/08/16 SpikeMix = Supelco LC20141V: 25 µl & Accu 216041125: 25 µl Pct Recovery = 78% Analysis Date = 08/26/16 SpikeMix = NSI 041816AVOC: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 74% Analysis Date = 08/12/16 SpikeMix = ChemService 5082900: 25 µl & Phenova B20160319: 25 µl Pct Recovery = 79% Analysis Date = 06/30/16 SpikeMix = Crescent 03FF058: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 74% Analysis Date = 03/06/15 SpikeMix = ERA 0227-14-06.1A: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 70% Analysis Date = 12/17/14 SpikeMix = Supelco LC06438: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 75% Analysis Date = 09/21/14 SpikeMix = Supelco LC06438: 20 µl Pct Recovery = 64% Analysis Date = 06/10/14 SpikeMix = NSI 032614: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 83% Analysis Date = 03/19/15 SpikeMix = Spex Organics C1140417015: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 77% Analysis Date = 11/22/14 SpikeMix = NSI 032614: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 71% Analysis Date = 08/19/14 SpikeMix = Spex Organics C1140417015: 20 µl & Accu 214031115: 20 µl Pct Recovery = 83% Analysis Date = 08/16/14 SpikeMix = ERA 0227-14-06.1A: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 79% Analysis Date = 09/29/15 SpikeMix = Accu 215041380: 25 µl & ERA 0406-15-03: 25 µl Pct Recovery = 84% Analysis Date = 08/15/15 SpikeMix = Supelco LC13545: 25 µl & Crescent 04EE008: 25 µl Pct Recovery = 91% Analysis Date = 07/13/15 SpikeMix = Crescent 04EE008: 25 µl & NSI 050515AVOC: 25 µl Pct Recovery = 73% Analysis Date = 11/29/16 SpikeMix = ChemService 5082900: 15 µl & Phenova B20160319: 15 µl Pct Recovery = 87% Analysis Date = 10/13/16 SpikeMix = NSI 041816AVOC: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 69% Analysis Date = 09/28/16 SpikeMix = Crescent 03FF058: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 75% Analysis Date = 06/30/16 SpikeMix = ChemService 5082900: 15 µl & Accu 216041125: 15 µl Pct Recovery = 77% Analysis Date = 06/10/16 SpikeMix = NSI 041816AVOC: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 80% Analysis Date = 05/27/16 SpikeMix = Phenova B20160319: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 84% Analysis Date = 04/02/16 SpikeMix = Supelco LC13545: 15 µl & Accu 215041380: 15 µl Pct Recovery = 67% Analysis Date = 03/04/16 SpikeMix = Accu 215041380: 15 µl & ERA 0406-15-03: 15 µl Pct Recovery = 60% Analysis Date = 06/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Accu 215041380: 15 µl Pct Recovery = 71% Analysis Date = 12/18/15 SpikeMix = Supelco LC13545: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 91% Analysis Date = 10/17/15 SpikeMix = Crescent 04EE008: 15 µl & NSI 050515AVOC: 15 µl Pct Recovery = 85% Analysis Date = 05/09/15 SpikeMix = Spex Organics EN150428007: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 76% Analysis Date = 10/21/14 SpikeMix = ERA 0227-14-06.1A: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 81% Analysis Date = 06/18/14 SpikeMix = Supelco LC06438: 10 µl & Accu 214031115: 10 µl Pct Recovery = 74% Analysis Date = 05/30/14 SpikeMix = NSI 032614: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 63% Analysis Date = 05/03/14 SpikeMix = Crescent 03DD004: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 76% Analysis Date = 11/06/14 SpikeMix = Spex Organics C1140417015: 10 µl & Crescent 03DD004: 10 µl Pct Recovery = 84% Analysis Date = 09/09/14 SpikeMix = NSI 032614: 10 µl & Spex Organics C1140417015: 10 µl Pct Recovery = 104% Analysis Date = 07/23/14 SpikeMix = Spex Organics C1140417015: 10 µl & Accu 214031115: 10 µl Pct Recovery = 75% Analysis Date = 07/11/14 SpikeMix = Spex Organics C1140417015: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 79% Analysis Date = 02/18/16 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 67% Analysis Date = 11/20/15 SpikeMix = Accu 215041380: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 90% Analysis Date = 11/12/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 77% Analysis Date = 05/21/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 80% Analysis Date = 05/13/16 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 80% Analysis Date = 01/27/16 SpikeMix = Crescent 04EE008: 10 µl & NSI 050515AVOC: 10 µl Pct Recovery = 77% Analysis Date = 08/07/15 SpikeMix = Crescent 04EE008: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 81% Analysis Date = 05/09/15 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 76% Analysis Date = 12/16/16 Pct Recovery = 80% Analysis Date = 12/11/16 Pct Recovery = 80% Analysis Date = 12/11/16 Pct Recovery = 80% Analysis Date = 12/06/16 Pct Recovery = 80% Analysis Date = 12/06/16 Pct Recovery = 80% Analysis Date = 12/01/16 Pct Recovery = 80% Analysis Date = 12/01/16 Pct Recovery = 80% Analysis Date = 11/26/16 Pct Recovery = 80% Analysis Date = 11/26/16 Pct Recovery = 80% Analysis Date = 11/22/16 Pct Recovery = 80% Analysis Date = 11/22/16 Pct Recovery = 80% Analysis Date = 11/17/16 Pct Recovery = 80% Analysis Date = 11/17/16 Pct Recovery = 80% Analysis Date = 11/12/16 Pct Recovery = 80% Analysis Date = 11/12/16 Pct Recovery = 80% Analysis Date = 11/07/16 Pct Recovery = 80% Analysis Date = 11/07/16 Pct Recovery = 80% Analysis Date = 11/02/16 Pct Recovery = 79% Analysis Date = 11/02/16 Pct Recovery = 79% Analysis Date = 10/29/16 Pct Recovery = 79% Analysis Date = 10/29/16 Pct Recovery = 79% Analysis Date = 10/24/16 Pct Recovery = 79% Analysis Date = 10/24/16 Pct Recovery = 79% Analysis Date = 10/19/16 Pct Recovery = 79% Analysis Date = 10/19/16 Pct Recovery = 79% Analysis Date = 10/14/16 Pct Recovery = 79% Analysis Date = 10/14/16 Pct Recovery = 79% Analysis Date = 10/09/16 Pct Recovery = 79% Analysis Date = 10/09/16 Pct Recovery = 79% Analysis Date = 10/05/16 Pct Recovery = 79% Analysis Date = 10/05/16 Pct Recovery = 79% Analysis Date = 09/30/16 Pct Recovery = 79% Analysis Date = 09/30/16 Pct Recovery = 79% Analysis Date = 09/25/16 Pct Recovery = 79% Analysis Date = 09/25/16 Pct Recovery = 79% Analysis Date = 09/20/16 Pct Recovery = 79% Analysis Date = 09/20/16 Pct Recovery = 79% Analysis Date = 09/15/16 Pct Recovery = 79% Analysis Date = 09/15/16 Pct Recovery = 79% Analysis Date = 09/11/16 Pct Recovery = 79% Analysis Date = 09/11/16 Pct Recovery = 79% Analysis Date = 09/06/16 Pct Recovery = 79% Analysis Date = 09/06/16 Pct Recovery = 79% Analysis Date = 09/01/16 Pct Recovery = 78% Analysis Date = 09/01/16 Pct Recovery = 78% Analysis Date = 08/27/16 Pct Recovery = 78% Analysis Date = 08/27/16 Pct Recovery = 78% Analysis Date = 08/23/16 Pct Recovery = 78% Analysis Date = 08/23/16 Pct Recovery = 78% Analysis Date = 08/18/16 Pct Recovery = 78% Analysis Date = 08/18/16 Pct Recovery = 78% Analysis Date = 08/13/16 Pct Recovery = 78% Analysis Date = 08/13/16 Pct Recovery = 78% Analysis Date = 08/08/16 Pct Recovery = 78% Analysis Date = 08/08/16 Pct Recovery = 78% Analysis Date = 08/03/16 Pct Recovery = 78% Analysis Date = 08/03/16 Pct Recovery = 78% Analysis Date = 07/30/16 Pct Recovery = 78% Analysis Date = 07/30/16 Pct Recovery = 78% Analysis Date = 07/25/16 Pct Recovery = 78% Analysis Date = 07/25/16 Pct Recovery = 78% Analysis Date = 07/20/16 Pct Recovery = 78% Analysis Date = 07/20/16 Pct Recovery = 78% Analysis Date = 07/15/16 Pct Recovery = 78% Analysis Date = 07/15/16 Pct Recovery = 78% Analysis Date = 07/10/16 Pct Recovery = 78% Analysis Date = 07/10/16 Pct Recovery = 78% Analysis Date = 07/06/16 Pct Recovery = 78% Analysis Date = 07/06/16 Pct Recovery = 78% Analysis Date = 07/01/16 Pct Recovery = 78% Analysis Date = 07/01/16 Pct Recovery = 78% Analysis Date = 06/26/16 Pct Recovery = 78% Analysis Date = 06/26/16 Pct Recovery = 78% Analysis Date = 06/21/16 Pct Recovery = 78% Analysis Date = 06/21/16 Pct Recovery = 78% Analysis Date = 06/16/16 Pct Recovery = 78% Analysis Date = 06/16/16 Pct Recovery = 78% Analysis Date = 06/12/16 Pct Recovery = 78% Analysis Date = 06/12/16 Pct Recovery = 78% Analysis Date = 06/07/16 Pct Recovery = 78% Analysis Date = 06/07/16 Pct Recovery = 78% Analysis Date = 06/02/16 Pct Recovery = 78% Analysis Date = 06/02/16 Pct Recovery = 78% Analysis Date = 05/28/16 Pct Recovery = 78% Analysis Date = 05/28/16 Pct Recovery = 78% Analysis Date = 05/24/16 Pct Recovery = 78% Analysis Date = 05/24/16 Pct Recovery = 78% Analysis Date = 05/19/16 Pct Recovery = 78% Analysis Date = 05/19/16 Pct Recovery = 78% Analysis Date = 05/14/16 Pct Recovery = 78% Analysis Date = 05/14/16 Pct Recovery = 78% Analysis Date = 05/09/16 Pct Recovery = 78% Analysis Date = 05/09/16 Pct Recovery = 78% Analysis Date = 05/04/16 Pct Recovery = 78% Analysis Date = 05/04/16 Pct Recovery = 78% Analysis Date = 04/30/16 Pct Recovery = 78% Analysis Date = 04/30/16 Pct Recovery = 78% Analysis Date = 04/25/16 Pct Recovery = 78% Analysis Date = 04/25/16 Pct Recovery = 78% Analysis Date = 04/20/16 Pct Recovery = 78% Analysis Date = 04/20/16 Pct Recovery = 78% Analysis Date = 04/15/16 Pct Recovery = 78% Analysis Date = 04/15/16 Pct Recovery = 78% Analysis Date = 04/10/16 Pct Recovery = 78% Analysis Date = 04/10/16 Pct Recovery = 78% Analysis Date = 04/06/16 Pct Recovery = 78% Analysis Date = 04/06/16 Pct Recovery = 78% Analysis Date = 04/01/16 Pct Recovery = 78% Analysis Date = 04/01/16 Pct Recovery = 78% Analysis Date = 03/27/16 Pct Recovery = 78% Analysis Date = 03/27/16 Pct Recovery = 78% Analysis Date = 03/22/16 Pct Recovery = 78% Analysis Date = 03/22/16 Pct Recovery = 78% Analysis Date = 03/17/16 Pct Recovery = 78% Analysis Date = 03/17/16 Pct Recovery = 78% Analysis Date = 03/13/16 Pct Recovery = 78% Analysis Date = 03/13/16 Pct Recovery = 78% Analysis Date = 03/08/16 Pct Recovery = 78% Analysis Date = 03/08/16 Pct Recovery = 78% Analysis Date = 03/03/16 Pct Recovery = 78% Analysis Date = 03/03/16 Pct Recovery = 78% Analysis Date = 02/27/16 Pct Recovery = 78% Analysis Date = 02/27/16 Pct Recovery = 78% Analysis Date = 02/23/16 Pct Recovery = 78% Analysis Date = 02/23/16 Pct Recovery = 78% Analysis Date = 02/18/16 Pct Recovery = 78% Analysis Date = 02/18/16 Pct Recovery = 78% Analysis Date = 02/13/16 Pct Recovery = 78% Analysis Date = 02/13/16 Pct Recovery = 78% Analysis Date = 02/08/16 Pct Recovery = 78% Analysis Date = 02/08/16 Pct Recovery = 78% Analysis Date = 02/03/16 Pct Recovery = 78% Analysis Date = 02/03/16 Pct Recovery = 78% Analysis Date = 01/30/16 Pct Recovery = 79% Analysis Date = 01/30/16 Pct Recovery = 79% Analysis Date = 01/25/16 Pct Recovery = 79% Analysis Date = 01/25/16 Pct Recovery = 79% Analysis Date = 01/20/16 Pct Recovery = 79% Analysis Date = 01/20/16 Pct Recovery = 79% Analysis Date = 01/15/16 Pct Recovery = 79% Analysis Date = 01/15/16 Pct Recovery = 79% Analysis Date = 01/10/16 Pct Recovery = 79% Analysis Date = 01/10/16 Pct Recovery = 79% Analysis Date = 01/06/16 Pct Recovery = 79% Analysis Date = 01/06/16 Pct Recovery = 79% Analysis Date = 01/01/16 Pct Recovery = 79% Analysis Date = 01/01/16 Pct Recovery = 79% Analysis Date = 12/27/15 Pct Recovery = 79% Analysis Date = 12/27/15 Pct Recovery = 79% Analysis Date = 12/22/15 Pct Recovery = 79% Analysis Date = 12/22/15 Pct Recovery = 79% Analysis Date = 12/17/15 Pct Recovery = 79% Analysis Date = 12/17/15 Pct Recovery = 79% Analysis Date = 12/13/15 Pct Recovery = 79% Analysis Date = 12/13/15 Pct Recovery = 79% Analysis Date = 12/08/15 Pct Recovery = 79% Analysis Date = 12/08/15 Pct Recovery = 79% Analysis Date = 12/03/15 Pct Recovery = 79% Analysis Date = 12/03/15 Pct Recovery = 79% Analysis Date = 11/28/15 Pct Recovery = 79% Analysis Date = 11/28/15 Pct Recovery = 79% Analysis Date = 11/24/15 Pct Recovery = 79% Analysis Date = 11/24/15 Pct Recovery = 79% Analysis Date = 11/19/15 Pct Recovery = 79% Analysis Date = 11/19/15 Pct Recovery = 79% Analysis Date = 11/14/15 Pct Recovery = 79% Analysis Date = 11/14/15 Pct Recovery = 79% Analysis Date = 11/09/15 Pct Recovery = 79% Analysis Date = 11/09/15 Pct Recovery = 79% Analysis Date = 11/04/15 Pct Recovery = 79% Analysis Date = 11/04/15 Pct Recovery = 79% Analysis Date = 10/31/15 Pct Recovery = 79% Analysis Date = 10/31/15 Pct Recovery = 79% Analysis Date = 10/26/15 Pct Recovery = 79% Analysis Date = 10/26/15 Pct Recovery = 79% Analysis Date = 10/21/15 Pct Recovery = 79% Analysis Date = 10/21/15 Pct Recovery = 79% Analysis Date = 10/16/15 Pct Recovery = 79% Analysis Date = 10/16/15 Pct Recovery = 79% Analysis Date = 10/11/15 Pct Recovery = 79% Analysis Date = 10/11/15 Pct Recovery = 79% Analysis Date = 10/07/15 Pct Recovery = 79% Analysis Date = 10/07/15 Pct Recovery = 79% Analysis Date = 10/02/15 Pct Recovery = 79% Analysis Date = 10/02/15 Pct Recovery = 79% Analysis Date = 09/27/15 Pct Recovery = 79% Analysis Date = 09/27/15 Pct Recovery = 79% Analysis Date = 09/22/15 Pct Recovery = 79% Analysis Date = 09/22/15 Pct Recovery = 79% Analysis Date = 09/17/15 Pct Recovery = 79% Analysis Date = 09/17/15 Pct Recovery = 79% Analysis Date = 09/13/15 Pct Recovery = 79% Analysis Date = 09/13/15 Pct Recovery = 79% Analysis Date = 09/08/15 Pct Recovery = 79% Analysis Date = 09/08/15 Pct Recovery = 79% Analysis Date = 09/03/15 Pct Recovery = 79% Analysis Date = 09/03/15 Pct Recovery = 79% Analysis Date = 08/29/15 Pct Recovery = 79% Analysis Date = 08/29/15 Pct Recovery = 79% Analysis Date = 08/25/15 Pct Recovery = 79% Analysis Date = 08/25/15 Pct Recovery = 79% Analysis Date = 08/20/15 Pct Recovery = 79% Analysis Date = 08/20/15 Pct Recovery = 79% Analysis Date = 08/15/15 Pct Recovery = 79% Analysis Date = 08/15/15 Pct Recovery = 79% Analysis Date = 08/10/15 Pct Recovery = 79% Analysis Date = 08/10/15 Pct Recovery = 79% Analysis Date = 08/05/15 Pct Recovery = 79% Analysis Date = 08/05/15 Pct Recovery = 79% Analysis Date = 08/01/15 Pct Recovery = 79% Analysis Date = 08/01/15 Pct Recovery = 79% Analysis Date = 07/27/15 Pct Recovery = 79% Analysis Date = 07/27/15 Pct Recovery = 79% Analysis Date = 07/22/15 Pct Recovery = 79% Analysis Date = 07/22/15 Pct Recovery = 79% Analysis Date = 07/17/15 Pct Recovery = 79% Analysis Date = 07/17/15 Pct Recovery = 79% Analysis Date = 07/12/15 Pct Recovery = 79% Analysis Date = 07/12/15 Pct Recovery = 79% Analysis Date = 07/08/15 Pct Recovery = 79% Analysis Date = 07/08/15 Pct Recovery = 79% Analysis Date = 07/03/15 Pct Recovery = 79% Analysis Date = 07/03/15 Pct Recovery = 79% Analysis Date = 06/28/15 Pct Recovery = 79% Analysis Date = 06/28/15 Pct Recovery = 79% Analysis Date = 06/23/15 Pct Recovery = 79% Analysis Date = 06/23/15 Pct Recovery = 79% Analysis Date = 06/18/15 Pct Recovery = 79% Analysis Date = 06/18/15 Pct Recovery = 79% Analysis Date = 06/14/15 Pct Recovery = 79% Analysis Date = 06/14/15 Pct Recovery = 79% Analysis Date = 06/09/15 Pct Recovery = 79% Analysis Date = 06/09/15 Pct Recovery = 79% Analysis Date = 06/04/15 Pct Recovery = 79% Analysis Date = 06/04/15 Pct Recovery = 79% Analysis Date = 05/30/15 Pct Recovery = 79% Analysis Date = 05/30/15 Pct Recovery = 79% Analysis Date = 05/25/15 Pct Recovery = 79% Analysis Date = 05/25/15 Pct Recovery = 79% Analysis Date = 05/21/15 Pct Recovery = 79% Analysis Date = 05/21/15 Pct Recovery = 79% Analysis Date = 05/16/15 Pct Recovery = 79% Analysis Date = 05/16/15 Pct Recovery = 79% Analysis Date = 05/11/15 Pct Recovery = 79% Analysis Date = 05/11/15 Pct Recovery = 79% Analysis Date = 05/06/15 Pct Recovery = 79% Analysis Date = 05/06/15 Pct Recovery = 79% Analysis Date = 05/02/15 Pct Recovery = 79% Analysis Date = 05/02/15 Pct Recovery = 79% Analysis Date = 04/27/15 Pct Recovery = 78% Analysis Date = 04/27/15 Pct Recovery = 78% Analysis Date = 04/22/15 Pct Recovery = 78% Analysis Date = 04/22/15 Pct Recovery = 78% Analysis Date = 04/17/15 Pct Recovery = 78% Analysis Date = 04/17/15 Pct Recovery = 78% Analysis Date = 04/12/15 Pct Recovery = 78% Analysis Date = 04/12/15 Pct Recovery = 78% Analysis Date = 04/08/15 Pct Recovery = 78% Analysis Date = 04/08/15 Pct Recovery = 78% Analysis Date = 04/03/15 Pct Recovery = 78% Analysis Date = 04/03/15 Pct Recovery = 78% Analysis Date = 03/29/15 Pct Recovery = 78% Analysis Date = 03/29/15 Pct Recovery = 78% Analysis Date = 03/24/15 Pct Recovery = 78% Analysis Date = 03/24/15 Pct Recovery = 78% Analysis Date = 03/19/15 Pct Recovery = 78% Analysis Date = 03/19/15 Pct Recovery = 78% Analysis Date = 03/15/15 Pct Recovery = 78% Analysis Date = 03/15/15 Pct Recovery = 78% Analysis Date = 03/10/15 Pct Recovery = 78% Analysis Date = 03/10/15 Pct Recovery = 78% Analysis Date = 03/05/15 Pct Recovery = 78% Analysis Date = 03/05/15 Pct Recovery = 78% Analysis Date = 02/28/15 Pct Recovery = 78% Analysis Date = 02/28/15 Pct Recovery = 78% Analysis Date = 02/23/15 Pct Recovery = 78% Analysis Date = 02/23/15 Pct Recovery = 78% Analysis Date = 02/19/15 Pct Recovery = 78% Analysis Date = 02/19/15 Pct Recovery = 78% Analysis Date = 02/14/15 Pct Recovery = 78% Analysis Date = 02/14/15 Pct Recovery = 78% Analysis Date = 02/09/15 Pct Recovery = 78% Analysis Date = 02/09/15 Pct Recovery = 78% Analysis Date = 02/04/15 Pct Recovery = 78% Analysis Date = 02/04/15 Pct Recovery = 78% Analysis Date = 01/31/15 Pct Recovery = 78% Analysis Date = 01/31/15 Pct Recovery = 78% Analysis Date = 01/26/15 Pct Recovery = 78% Analysis Date = 01/26/15 Pct Recovery = 78% Analysis Date = 01/21/15 Pct Recovery = 78% Analysis Date = 01/21/15 Pct Recovery = 78% Analysis Date = 01/16/15 Pct Recovery = 78% Analysis Date = 01/16/15 Pct Recovery = 78% Analysis Date = 01/11/15 Pct Recovery = 78% Analysis Date = 01/11/15 Pct Recovery = 78% Analysis Date = 01/07/15 Pct Recovery = 78% Analysis Date = 01/07/15 Pct Recovery = 78% Analysis Date = 01/02/15 Pct Recovery = 78% Analysis Date = 01/02/15 Pct Recovery = 78% Analysis Date = 12/28/14 Pct Recovery = 78% Analysis Date = 12/28/14 Pct Recovery = 78% Analysis Date = 12/23/14 Pct Recovery = 78% Analysis Date = 12/23/14 Pct Recovery = 78% Analysis Date = 12/18/14 Pct Recovery = 78% Analysis Date = 12/18/14 Pct Recovery = 78% Analysis Date = 12/14/14 Pct Recovery = 78% Analysis Date = 12/14/14 Pct Recovery = 78% Analysis Date = 12/09/14 Pct Recovery = 78% Analysis Date = 12/09/14 Pct Recovery = 78% Analysis Date = 12/04/14 Pct Recovery = 78% Analysis Date = 12/04/14 Pct Recovery = 78% Analysis Date = 11/29/14 Pct Recovery = 78% Analysis Date = 11/29/14 Pct Recovery = 78% Analysis Date = 11/24/14 Pct Recovery = 78% Analysis Date = 11/24/14 Pct Recovery = 78% Analysis Date = 11/20/14 Pct Recovery = 78% Analysis Date = 11/20/14 Pct Recovery = 78% Analysis Date = 11/15/14 Pct Recovery = 78% Analysis Date = 11/15/14 Pct Recovery = 78% Analysis Date = 11/10/14 Pct Recovery = 78% Analysis Date = 11/10/14 Pct Recovery = 78% Analysis Date = 11/05/14 Pct Recovery = 78% Analysis Date = 11/05/14 Pct Recovery = 78% Analysis Date = 11/01/14 Pct Recovery = 78% Analysis Date = 11/01/14 Pct Recovery = 78% Analysis Date = 10/27/14 Pct Recovery = 78% Analysis Date = 10/27/14 Pct Recovery = 78% Analysis Date = 10/22/14 Pct Recovery = 78% Analysis Date = 10/22/14 Pct Recovery = 78% Analysis Date = 10/17/14 Pct Recovery = 78% Analysis Date = 10/17/14 Pct Recovery = 78% Analysis Date = 10/12/14 Pct Recovery = 77% Analysis Date = 10/12/14 Pct Recovery = 77% Analysis Date = 10/08/14 Pct Recovery = 77% Analysis Date = 10/08/14 Pct Recovery = 77% Analysis Date = 10/03/14 Pct Recovery = 77% Analysis Date = 10/03/14 Pct Recovery = 77% Analysis Date = 09/28/14 Pct Recovery = 77% Analysis Date = 09/28/14 Pct Recovery = 77% Analysis Date = 09/23/14 Pct Recovery = 77% Analysis Date = 09/23/14 Pct Recovery = 77% Analysis Date = 09/18/14 Pct Recovery = 77% Analysis Date = 09/18/14 Pct Recovery = 77% Analysis Date = 09/14/14 Pct Recovery = 77% Analysis Date = 09/14/14 Pct Recovery = 77% Analysis Date = 09/09/14 Pct Recovery = 77% Analysis Date = 09/09/14 Pct Recovery = 77% Analysis Date = 09/04/14 Pct Recovery = 77% Analysis Date = 09/04/14 Pct Recovery = 77% Analysis Date = 08/30/14 Pct Recovery = 77% Analysis Date = 08/30/14 Pct Recovery = 77% Analysis Date = 08/25/14 Pct Recovery = 77% Analysis Date = 08/25/14 Pct Recovery = 77% Analysis Date = 08/21/14 Pct Recovery = 77% Analysis Date = 08/21/14 Pct Recovery = 77% Analysis Date = 08/16/14 Pct Recovery = 77% Analysis Date = 08/16/14 Pct Recovery = 77% Analysis Date = 08/11/14 Pct Recovery = 77% Analysis Date = 08/11/14 Pct Recovery = 77% Analysis Date = 08/06/14 Pct Recovery = 77% Analysis Date = 08/06/14 Pct Recovery = 77% Analysis Date = 08/02/14 Pct Recovery = 77% Analysis Date = 08/02/14 Pct Recovery = 77% Analysis Date = 07/28/14 Pct Recovery = 77% Analysis Date = 07/28/14 Pct Recovery = 77% Analysis Date = 07/23/14 Pct Recovery = 77% Analysis Date = 07/23/14 Pct Recovery = 77% Analysis Date = 07/18/14 Pct Recovery = 77% Analysis Date = 07/18/14 Pct Recovery = 77% Analysis Date = 07/13/14 Pct Recovery = 77% Analysis Date = 07/13/14 Pct Recovery = 77% Analysis Date = 07/09/14 Pct Recovery = 77% Analysis Date = 07/09/14 Pct Recovery = 77% Analysis Date = 07/04/14 Pct Recovery = 77% Analysis Date = 07/04/14 Pct Recovery = 77% Analysis Date = 06/29/14 Pct Recovery = 77% Analysis Date = 06/29/14 Pct Recovery = 77% Analysis Date = 06/24/14 Pct Recovery = 77% Analysis Date = 06/24/14 Pct Recovery = 77% Analysis Date = 06/19/14 Pct Recovery = 77% Analysis Date = 06/19/14 Pct Recovery = 77% Analysis Date = 06/15/14 Pct Recovery = 77% Analysis Date = 06/15/14 Pct Recovery = 77% Analysis Date = 06/10/14 Pct Recovery = 77% Analysis Date = 06/10/14 Pct Recovery = 77% Analysis Date = 06/05/14 Pct Recovery = 77% Analysis Date = 06/05/14 Pct Recovery = 77% Analysis Date = 05/31/14 Pct Recovery = 77% Analysis Date = 05/31/14 Pct Recovery = 77% Analysis Date = 05/26/14 Pct Recovery = 77% Analysis Date = 05/26/14 Pct Recovery = 77% Analysis Date = 05/22/14 Pct Recovery = 77% Analysis Date = 05/22/14 Pct Recovery = 77% Analysis Date = 05/17/14 Pct Recovery = 77% Analysis Date = 05/17/14 Pct Recovery = 77% Analysis Date = 05/12/14 Pct Recovery = 77% Analysis Date = 05/12/14 Pct Recovery = 77% Analysis Date = 05/07/14 Pct Recovery = 77% Analysis Date = 05/07/14 Pct Recovery = 77% Analysis Date = 05/03/14 Pct Recovery = 77% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
NAPHTHALENE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 47 78% 8% 77% 7%
Total 47 78% 8% 77% 7%

Sample Statistics
NAPHTHALENE

Characteristic N % % Basis
Plotted 47 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 47 .  
False Negatives 0 0% 0 out of 47
Not Spiked 26 .  
False Positives 0 0% 0 out of 26

BQS OBSP Determination:
NUMBER OF TENTATIVELY IDENTIFIED COMPOUNDS (TICS)
METHOD: 4440 , TESTIDCODE: 99871GCM66
Open Data Set

The SGPlot Procedure

Sample Statistics
NUMBER OF TENTATIVELY IDENTIFIED COMPOUNDS (TICS)

Characteristic N % % Basis
Plotted 0 . Spiked
Estimated Values 0 . Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 . Spiked
Spiked 0 .  
False Negatives 0 . 0 out of 0
Not Spiked 73 .  
False Positives 2 3% 2 out of 73

BQS OBSP Determination:
O-ETHYL TOLUENE
METHOD: 4440 , TESTIDCODE: 77220GCM66
Open Data Set

Analysis Date = 12/16/16 SpikeMix = NSI 041816AVOC: 40 µl & ChemService 5082900: 40 µl Pct Recovery = 83% Analysis Date = 12/12/16 SpikeMix = Accu 216041125: 40 µl & Crescent 03FF058: 40 µl Pct Recovery = 93% Analysis Date = 08/04/16 SpikeMix = Crescent 03FF058: 40 µl & Supelco LC20141V: 40 µl Pct Recovery = 79% Analysis Date = 07/14/16 SpikeMix = Accu 216041125: 40 µl & NSI 041816AVOC: 40 µl Pct Recovery = 89% Analysis Date = 11/21/16 SpikeMix = Crescent 03FF058: 25 µl & Supelco LC20141V: 25 µl Pct Recovery = 82% Analysis Date = 08/26/16 SpikeMix = NSI 041816AVOC: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 78% Analysis Date = 06/30/16 SpikeMix = Crescent 03FF058: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 79% Analysis Date = 06/21/16 SpikeMix = Phenova B20160319: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 89% Analysis Date = 05/24/16 SpikeMix = Accu 216041125: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 81% Analysis Date = 11/22/14 SpikeMix = NSI 032614: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 93% Analysis Date = 06/10/14 SpikeMix = Crescent 03DD004: 20 µl & NSI 032614: 20 µl Pct Recovery = 81% Analysis Date = 06/10/14 SpikeMix = NSI 032614: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 91% Analysis Date = 05/01/14 SpikeMix = Accu 214031115: 20 µl & NSI 032614: 20 µl Pct Recovery = 77% Analysis Date = 04/09/15 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 89% Analysis Date = 03/06/15 SpikeMix = ERA 0227-14-06.1A: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 90% Analysis Date = 11/14/14 SpikeMix = Crescent 03DD004: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 84% Analysis Date = 08/16/14 SpikeMix = ERA 0227-14-06.1A: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 91% Analysis Date = 07/01/14 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 81% Analysis Date = 08/15/15 SpikeMix = Supelco LC13545: 25 µl & Crescent 04EE008: 25 µl Pct Recovery = 94% Analysis Date = 06/16/15 SpikeMix = ERA 0406-15-03: 25 µl & Supelco LC13545: 25 µl Pct Recovery = 87% Analysis Date = 10/13/16 SpikeMix = Accu 216041125: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 90% Analysis Date = 10/13/16 SpikeMix = NSI 041816AVOC: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 79% Analysis Date = 09/28/16 SpikeMix = Crescent 03FF058: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 75% Analysis Date = 09/08/16 SpikeMix = Phenova B20160319: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 74% Analysis Date = 08/20/16 SpikeMix = Accu 216041125: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 84% Analysis Date = 07/29/16 SpikeMix = Phenova B20160319: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 87% Analysis Date = 06/10/16 SpikeMix = NSI 041816AVOC: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 84% Analysis Date = 04/26/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 87% Analysis Date = 02/05/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 92% Analysis Date = 11/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 94% Analysis Date = 10/16/15 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 93% Analysis Date = 05/09/15 SpikeMix = Spex Organics EN150428007: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 108% Analysis Date = 04/02/16 SpikeMix = Supelco LC13545: 15 µl & Accu 215041380: 15 µl Pct Recovery = 86% Analysis Date = 12/18/15 SpikeMix = Supelco LC13545: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 91% Analysis Date = 09/09/14 SpikeMix = Accu 214031115: 10 µl & NSI 032614: 10 µl Pct Recovery = 113% Analysis Date = 09/09/14 SpikeMix = NSI 032614: 10 µl & Spex Organics C1140417015: 10 µl Pct Recovery = 114% Analysis Date = 07/29/14 SpikeMix = Crescent 03DD004: 10 µl & NSI 032614: 10 µl Pct Recovery = 92% Analysis Date = 05/30/14 SpikeMix = NSI 032614: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 74% Analysis Date = 01/13/15 SpikeMix = Accu 214031115: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 88% Analysis Date = 10/21/14 SpikeMix = ERA 0227-14-06.1A: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 92% Analysis Date = 10/04/14 SpikeMix = Crescent 03DD004: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 88% Analysis Date = 07/11/14 SpikeMix = Spex Organics C1140417015: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 96% Analysis Date = 02/18/16 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 95% Analysis Date = 11/12/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 108% Analysis Date = 09/03/15 SpikeMix = NSI 050515AVOC: 10 µl & Spex Organics EN150428007: 10 µl Pct Recovery = 83% Analysis Date = 05/21/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 115% Analysis Date = 05/13/16 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 98% Analysis Date = 03/17/16 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 78% Analysis Date = 12/10/15 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 93% Analysis Date = 06/27/15 SpikeMix = ERA 0406-15-03: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 95% Analysis Date = 05/09/15 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 102% Analysis Date = 12/15/16 Pct Recovery = 81% Analysis Date = 12/11/16 Pct Recovery = 81% Analysis Date = 12/11/16 Pct Recovery = 81% Analysis Date = 12/06/16 Pct Recovery = 81% Analysis Date = 12/06/16 Pct Recovery = 81% Analysis Date = 12/01/16 Pct Recovery = 81% Analysis Date = 12/01/16 Pct Recovery = 81% Analysis Date = 11/26/16 Pct Recovery = 81% Analysis Date = 11/26/16 Pct Recovery = 81% Analysis Date = 11/21/16 Pct Recovery = 82% Analysis Date = 11/21/16 Pct Recovery = 82% Analysis Date = 11/17/16 Pct Recovery = 82% Analysis Date = 11/17/16 Pct Recovery = 82% Analysis Date = 11/12/16 Pct Recovery = 82% Analysis Date = 11/12/16 Pct Recovery = 82% Analysis Date = 11/07/16 Pct Recovery = 82% Analysis Date = 11/07/16 Pct Recovery = 82% Analysis Date = 11/02/16 Pct Recovery = 82% Analysis Date = 11/02/16 Pct Recovery = 82% Analysis Date = 10/28/16 Pct Recovery = 82% Analysis Date = 10/28/16 Pct Recovery = 82% Analysis Date = 10/24/16 Pct Recovery = 82% Analysis Date = 10/24/16 Pct Recovery = 82% Analysis Date = 10/19/16 Pct Recovery = 82% Analysis Date = 10/19/16 Pct Recovery = 82% Analysis Date = 10/14/16 Pct Recovery = 82% Analysis Date = 10/14/16 Pct Recovery = 82% Analysis Date = 10/09/16 Pct Recovery = 83% Analysis Date = 10/09/16 Pct Recovery = 83% Analysis Date = 10/04/16 Pct Recovery = 83% Analysis Date = 10/04/16 Pct Recovery = 83% Analysis Date = 09/30/16 Pct Recovery = 83% Analysis Date = 09/30/16 Pct Recovery = 83% Analysis Date = 09/25/16 Pct Recovery = 83% Analysis Date = 09/25/16 Pct Recovery = 83% Analysis Date = 09/20/16 Pct Recovery = 83% Analysis Date = 09/20/16 Pct Recovery = 83% Analysis Date = 09/15/16 Pct Recovery = 83% Analysis Date = 09/15/16 Pct Recovery = 83% Analysis Date = 09/10/16 Pct Recovery = 83% Analysis Date = 09/10/16 Pct Recovery = 83% Analysis Date = 09/06/16 Pct Recovery = 83% Analysis Date = 09/06/16 Pct Recovery = 83% Analysis Date = 09/01/16 Pct Recovery = 84% Analysis Date = 09/01/16 Pct Recovery = 84% Analysis Date = 08/27/16 Pct Recovery = 84% Analysis Date = 08/27/16 Pct Recovery = 84% Analysis Date = 08/22/16 Pct Recovery = 84% Analysis Date = 08/22/16 Pct Recovery = 84% Analysis Date = 08/17/16 Pct Recovery = 84% Analysis Date = 08/17/16 Pct Recovery = 84% Analysis Date = 08/13/16 Pct Recovery = 84% Analysis Date = 08/13/16 Pct Recovery = 84% Analysis Date = 08/08/16 Pct Recovery = 84% Analysis Date = 08/08/16 Pct Recovery = 84% Analysis Date = 08/03/16 Pct Recovery = 84% Analysis Date = 08/03/16 Pct Recovery = 84% Analysis Date = 07/29/16 Pct Recovery = 84% Analysis Date = 07/29/16 Pct Recovery = 84% Analysis Date = 07/24/16 Pct Recovery = 85% Analysis Date = 07/24/16 Pct Recovery = 85% Analysis Date = 07/20/16 Pct Recovery = 85% Analysis Date = 07/20/16 Pct Recovery = 85% Analysis Date = 07/15/16 Pct Recovery = 85% Analysis Date = 07/15/16 Pct Recovery = 85% Analysis Date = 07/10/16 Pct Recovery = 85% Analysis Date = 07/10/16 Pct Recovery = 85% Analysis Date = 07/05/16 Pct Recovery = 85% Analysis Date = 07/05/16 Pct Recovery = 85% Analysis Date = 06/30/16 Pct Recovery = 85% Analysis Date = 06/30/16 Pct Recovery = 85% Analysis Date = 06/26/16 Pct Recovery = 85% Analysis Date = 06/26/16 Pct Recovery = 85% Analysis Date = 06/21/16 Pct Recovery = 86% Analysis Date = 06/21/16 Pct Recovery = 86% Analysis Date = 06/16/16 Pct Recovery = 86% Analysis Date = 06/16/16 Pct Recovery = 86% Analysis Date = 06/11/16 Pct Recovery = 86% Analysis Date = 06/11/16 Pct Recovery = 86% Analysis Date = 06/06/16 Pct Recovery = 86% Analysis Date = 06/06/16 Pct Recovery = 86% Analysis Date = 06/02/16 Pct Recovery = 86% Analysis Date = 06/02/16 Pct Recovery = 86% Analysis Date = 05/28/16 Pct Recovery = 86% Analysis Date = 05/28/16 Pct Recovery = 86% Analysis Date = 05/23/16 Pct Recovery = 86% Analysis Date = 05/23/16 Pct Recovery = 86% Analysis Date = 05/18/16 Pct Recovery = 87% Analysis Date = 05/18/16 Pct Recovery = 87% Analysis Date = 05/13/16 Pct Recovery = 87% Analysis Date = 05/13/16 Pct Recovery = 87% Analysis Date = 05/09/16 Pct Recovery = 87% Analysis Date = 05/09/16 Pct Recovery = 87% Analysis Date = 05/04/16 Pct Recovery = 87% Analysis Date = 05/04/16 Pct Recovery = 87% Analysis Date = 04/29/16 Pct Recovery = 87% Analysis Date = 04/29/16 Pct Recovery = 87% Analysis Date = 04/24/16 Pct Recovery = 87% Analysis Date = 04/24/16 Pct Recovery = 87% Analysis Date = 04/19/16 Pct Recovery = 88% Analysis Date = 04/19/16 Pct Recovery = 88% Analysis Date = 04/15/16 Pct Recovery = 88% Analysis Date = 04/15/16 Pct Recovery = 88% Analysis Date = 04/10/16 Pct Recovery = 88% Analysis Date = 04/10/16 Pct Recovery = 88% Analysis Date = 04/05/16 Pct Recovery = 88% Analysis Date = 04/05/16 Pct Recovery = 88% Analysis Date = 03/31/16 Pct Recovery = 88% Analysis Date = 03/31/16 Pct Recovery = 88% Analysis Date = 03/26/16 Pct Recovery = 88% Analysis Date = 03/26/16 Pct Recovery = 88% Analysis Date = 03/22/16 Pct Recovery = 89% Analysis Date = 03/22/16 Pct Recovery = 89% Analysis Date = 03/17/16 Pct Recovery = 89% Analysis Date = 03/17/16 Pct Recovery = 89% Analysis Date = 03/12/16 Pct Recovery = 89% Analysis Date = 03/12/16 Pct Recovery = 89% Analysis Date = 03/07/16 Pct Recovery = 89% Analysis Date = 03/07/16 Pct Recovery = 89% Analysis Date = 03/02/16 Pct Recovery = 89% Analysis Date = 03/02/16 Pct Recovery = 89% Analysis Date = 02/27/16 Pct Recovery = 89% Analysis Date = 02/27/16 Pct Recovery = 89% Analysis Date = 02/22/16 Pct Recovery = 90% Analysis Date = 02/22/16 Pct Recovery = 90% Analysis Date = 02/17/16 Pct Recovery = 90% Analysis Date = 02/17/16 Pct Recovery = 90% Analysis Date = 02/12/16 Pct Recovery = 90% Analysis Date = 02/12/16 Pct Recovery = 90% Analysis Date = 02/07/16 Pct Recovery = 90% Analysis Date = 02/07/16 Pct Recovery = 90% Analysis Date = 02/03/16 Pct Recovery = 90% Analysis Date = 02/03/16 Pct Recovery = 90% Analysis Date = 01/29/16 Pct Recovery = 90% Analysis Date = 01/29/16 Pct Recovery = 90% Analysis Date = 01/24/16 Pct Recovery = 91% Analysis Date = 01/24/16 Pct Recovery = 91% Analysis Date = 01/19/16 Pct Recovery = 91% Analysis Date = 01/19/16 Pct Recovery = 91% Analysis Date = 01/14/16 Pct Recovery = 91% Analysis Date = 01/14/16 Pct Recovery = 91% Analysis Date = 01/10/16 Pct Recovery = 91% Analysis Date = 01/10/16 Pct Recovery = 91% Analysis Date = 01/05/16 Pct Recovery = 91% Analysis Date = 01/05/16 Pct Recovery = 91% Analysis Date = 12/31/15 Pct Recovery = 91% Analysis Date = 12/31/15 Pct Recovery = 91% Analysis Date = 12/26/15 Pct Recovery = 92% Analysis Date = 12/26/15 Pct Recovery = 92% Analysis Date = 12/21/15 Pct Recovery = 92% Analysis Date = 12/21/15 Pct Recovery = 92% Analysis Date = 12/17/15 Pct Recovery = 92% Analysis Date = 12/17/15 Pct Recovery = 92% Analysis Date = 12/12/15 Pct Recovery = 92% Analysis Date = 12/12/15 Pct Recovery = 92% Analysis Date = 12/07/15 Pct Recovery = 92% Analysis Date = 12/07/15 Pct Recovery = 92% Analysis Date = 12/02/15 Pct Recovery = 92% Analysis Date = 12/02/15 Pct Recovery = 92% Analysis Date = 11/27/15 Pct Recovery = 92% Analysis Date = 11/27/15 Pct Recovery = 92% Analysis Date = 11/23/15 Pct Recovery = 93% Analysis Date = 11/23/15 Pct Recovery = 93% Analysis Date = 11/18/15 Pct Recovery = 93% Analysis Date = 11/18/15 Pct Recovery = 93% Analysis Date = 11/13/15 Pct Recovery = 93% Analysis Date = 11/13/15 Pct Recovery = 93% Analysis Date = 11/08/15 Pct Recovery = 93% Analysis Date = 11/08/15 Pct Recovery = 93% Analysis Date = 11/03/15 Pct Recovery = 93% Analysis Date = 11/03/15 Pct Recovery = 93% Analysis Date = 10/30/15 Pct Recovery = 93% Analysis Date = 10/30/15 Pct Recovery = 93% Analysis Date = 10/25/15 Pct Recovery = 93% Analysis Date = 10/25/15 Pct Recovery = 93% Analysis Date = 10/20/15 Pct Recovery = 93% Analysis Date = 10/20/15 Pct Recovery = 93% Analysis Date = 10/15/15 Pct Recovery = 93% Analysis Date = 10/15/15 Pct Recovery = 93% Analysis Date = 10/10/15 Pct Recovery = 93% Analysis Date = 10/10/15 Pct Recovery = 93% Analysis Date = 10/06/15 Pct Recovery = 94% Analysis Date = 10/06/15 Pct Recovery = 94% Analysis Date = 10/01/15 Pct Recovery = 94% Analysis Date = 10/01/15 Pct Recovery = 94% Analysis Date = 09/26/15 Pct Recovery = 94% Analysis Date = 09/26/15 Pct Recovery = 94% Analysis Date = 09/21/15 Pct Recovery = 94% Analysis Date = 09/21/15 Pct Recovery = 94% Analysis Date = 09/16/15 Pct Recovery = 94% Analysis Date = 09/16/15 Pct Recovery = 94% Analysis Date = 09/12/15 Pct Recovery = 94% Analysis Date = 09/12/15 Pct Recovery = 94% Analysis Date = 09/07/15 Pct Recovery = 94% Analysis Date = 09/07/15 Pct Recovery = 94% Analysis Date = 09/02/15 Pct Recovery = 94% Analysis Date = 09/02/15 Pct Recovery = 94% Analysis Date = 08/28/15 Pct Recovery = 94% Analysis Date = 08/28/15 Pct Recovery = 94% Analysis Date = 08/23/15 Pct Recovery = 94% Analysis Date = 08/23/15 Pct Recovery = 94% Analysis Date = 08/19/15 Pct Recovery = 94% Analysis Date = 08/19/15 Pct Recovery = 94% Analysis Date = 08/14/15 Pct Recovery = 94% Analysis Date = 08/14/15 Pct Recovery = 94% Analysis Date = 08/09/15 Pct Recovery = 94% Analysis Date = 08/09/15 Pct Recovery = 94% Analysis Date = 08/04/15 Pct Recovery = 94% Analysis Date = 08/04/15 Pct Recovery = 94% Analysis Date = 07/30/15 Pct Recovery = 94% Analysis Date = 07/30/15 Pct Recovery = 94% Analysis Date = 07/26/15 Pct Recovery = 94% Analysis Date = 07/26/15 Pct Recovery = 94% Analysis Date = 07/21/15 Pct Recovery = 94% Analysis Date = 07/21/15 Pct Recovery = 94% Analysis Date = 07/16/15 Pct Recovery = 94% Analysis Date = 07/16/15 Pct Recovery = 94% Analysis Date = 07/11/15 Pct Recovery = 94% Analysis Date = 07/11/15 Pct Recovery = 94% Analysis Date = 07/06/15 Pct Recovery = 95% Analysis Date = 07/06/15 Pct Recovery = 95% Analysis Date = 07/02/15 Pct Recovery = 95% Analysis Date = 07/02/15 Pct Recovery = 95% Analysis Date = 06/27/15 Pct Recovery = 95% Analysis Date = 06/27/15 Pct Recovery = 95% Analysis Date = 06/22/15 Pct Recovery = 95% Analysis Date = 06/22/15 Pct Recovery = 95% Analysis Date = 06/17/15 Pct Recovery = 95% Analysis Date = 06/17/15 Pct Recovery = 95% Analysis Date = 06/12/15 Pct Recovery = 95% Analysis Date = 06/12/15 Pct Recovery = 95% Analysis Date = 06/08/15 Pct Recovery = 95% Analysis Date = 06/08/15 Pct Recovery = 95% Analysis Date = 06/03/15 Pct Recovery = 95% Analysis Date = 06/03/15 Pct Recovery = 95% Analysis Date = 05/29/15 Pct Recovery = 95% Analysis Date = 05/29/15 Pct Recovery = 95% Analysis Date = 05/24/15 Pct Recovery = 95% Analysis Date = 05/24/15 Pct Recovery = 95% Analysis Date = 05/19/15 Pct Recovery = 95% Analysis Date = 05/19/15 Pct Recovery = 95% Analysis Date = 05/15/15 Pct Recovery = 95% Analysis Date = 05/15/15 Pct Recovery = 95% Analysis Date = 05/10/15 Pct Recovery = 95% Analysis Date = 05/10/15 Pct Recovery = 95% Analysis Date = 05/05/15 Pct Recovery = 95% Analysis Date = 05/05/15 Pct Recovery = 95% Analysis Date = 04/30/15 Pct Recovery = 95% Analysis Date = 04/30/15 Pct Recovery = 95% Analysis Date = 04/25/15 Pct Recovery = 95% Analysis Date = 04/25/15 Pct Recovery = 95% Analysis Date = 04/21/15 Pct Recovery = 95% Analysis Date = 04/21/15 Pct Recovery = 95% Analysis Date = 04/16/15 Pct Recovery = 95% Analysis Date = 04/16/15 Pct Recovery = 95% Analysis Date = 04/11/15 Pct Recovery = 95% Analysis Date = 04/11/15 Pct Recovery = 95% Analysis Date = 04/06/15 Pct Recovery = 95% Analysis Date = 04/06/15 Pct Recovery = 95% Analysis Date = 04/01/15 Pct Recovery = 95% Analysis Date = 04/01/15 Pct Recovery = 95% Analysis Date = 03/28/15 Pct Recovery = 95% Analysis Date = 03/28/15 Pct Recovery = 95% Analysis Date = 03/23/15 Pct Recovery = 95% Analysis Date = 03/23/15 Pct Recovery = 95% Analysis Date = 03/18/15 Pct Recovery = 95% Analysis Date = 03/18/15 Pct Recovery = 95% Analysis Date = 03/13/15 Pct Recovery = 95% Analysis Date = 03/13/15 Pct Recovery = 95% Analysis Date = 03/08/15 Pct Recovery = 95% Analysis Date = 03/08/15 Pct Recovery = 95% Analysis Date = 03/04/15 Pct Recovery = 95% Analysis Date = 03/04/15 Pct Recovery = 95% Analysis Date = 02/27/15 Pct Recovery = 94% Analysis Date = 02/27/15 Pct Recovery = 94% Analysis Date = 02/22/15 Pct Recovery = 94% Analysis Date = 02/22/15 Pct Recovery = 94% Analysis Date = 02/17/15 Pct Recovery = 94% Analysis Date = 02/17/15 Pct Recovery = 94% Analysis Date = 02/12/15 Pct Recovery = 94% Analysis Date = 02/12/15 Pct Recovery = 94% Analysis Date = 02/08/15 Pct Recovery = 94% Analysis Date = 02/08/15 Pct Recovery = 94% Analysis Date = 02/03/15 Pct Recovery = 94% Analysis Date = 02/03/15 Pct Recovery = 94% Analysis Date = 01/29/15 Pct Recovery = 94% Analysis Date = 01/29/15 Pct Recovery = 94% Analysis Date = 01/24/15 Pct Recovery = 94% Analysis Date = 01/24/15 Pct Recovery = 94% Analysis Date = 01/19/15 Pct Recovery = 94% Analysis Date = 01/19/15 Pct Recovery = 94% Analysis Date = 01/15/15 Pct Recovery = 94% Analysis Date = 01/15/15 Pct Recovery = 94% Analysis Date = 01/10/15 Pct Recovery = 94% Analysis Date = 01/10/15 Pct Recovery = 94% Analysis Date = 01/05/15 Pct Recovery = 93% Analysis Date = 01/05/15 Pct Recovery = 93% Analysis Date = 12/31/14 Pct Recovery = 93% Analysis Date = 12/31/14 Pct Recovery = 93% Analysis Date = 12/26/14 Pct Recovery = 93% Analysis Date = 12/26/14 Pct Recovery = 93% Analysis Date = 12/22/14 Pct Recovery = 93% Analysis Date = 12/22/14 Pct Recovery = 93% Analysis Date = 12/17/14 Pct Recovery = 93% Analysis Date = 12/17/14 Pct Recovery = 93% Analysis Date = 12/12/14 Pct Recovery = 93% Analysis Date = 12/12/14 Pct Recovery = 93% Analysis Date = 12/07/14 Pct Recovery = 93% Analysis Date = 12/07/14 Pct Recovery = 93% Analysis Date = 12/02/14 Pct Recovery = 93% Analysis Date = 12/02/14 Pct Recovery = 93% Analysis Date = 11/28/14 Pct Recovery = 93% Analysis Date = 11/28/14 Pct Recovery = 93% Analysis Date = 11/23/14 Pct Recovery = 93% Analysis Date = 11/23/14 Pct Recovery = 93% Analysis Date = 11/18/14 Pct Recovery = 93% Analysis Date = 11/18/14 Pct Recovery = 93% Analysis Date = 11/13/14 Pct Recovery = 92% Analysis Date = 11/13/14 Pct Recovery = 92% Analysis Date = 11/08/14 Pct Recovery = 92% Analysis Date = 11/08/14 Pct Recovery = 92% Analysis Date = 11/04/14 Pct Recovery = 92% Analysis Date = 11/04/14 Pct Recovery = 92% Analysis Date = 10/30/14 Pct Recovery = 92% Analysis Date = 10/30/14 Pct Recovery = 92% Analysis Date = 10/25/14 Pct Recovery = 92% Analysis Date = 10/25/14 Pct Recovery = 92% Analysis Date = 10/20/14 Pct Recovery = 92% Analysis Date = 10/20/14 Pct Recovery = 92% Analysis Date = 10/15/14 Pct Recovery = 92% Analysis Date = 10/15/14 Pct Recovery = 92% Analysis Date = 10/11/14 Pct Recovery = 92% Analysis Date = 10/11/14 Pct Recovery = 92% Analysis Date = 10/06/14 Pct Recovery = 91% Analysis Date = 10/06/14 Pct Recovery = 91% Analysis Date = 10/01/14 Pct Recovery = 91% Analysis Date = 10/01/14 Pct Recovery = 91% Analysis Date = 09/26/14 Pct Recovery = 91% Analysis Date = 09/26/14 Pct Recovery = 91% Analysis Date = 09/21/14 Pct Recovery = 91% Analysis Date = 09/21/14 Pct Recovery = 91% Analysis Date = 09/17/14 Pct Recovery = 91% Analysis Date = 09/17/14 Pct Recovery = 91% Analysis Date = 09/12/14 Pct Recovery = 91% Analysis Date = 09/12/14 Pct Recovery = 91% Analysis Date = 09/07/14 Pct Recovery = 91% Analysis Date = 09/07/14 Pct Recovery = 91% Analysis Date = 09/02/14 Pct Recovery = 90% Analysis Date = 09/02/14 Pct Recovery = 90% Analysis Date = 08/28/14 Pct Recovery = 90% Analysis Date = 08/28/14 Pct Recovery = 90% Analysis Date = 08/24/14 Pct Recovery = 90% Analysis Date = 08/24/14 Pct Recovery = 90% Analysis Date = 08/19/14 Pct Recovery = 90% Analysis Date = 08/19/14 Pct Recovery = 90% Analysis Date = 08/14/14 Pct Recovery = 90% Analysis Date = 08/14/14 Pct Recovery = 90% Analysis Date = 08/09/14 Pct Recovery = 90% Analysis Date = 08/09/14 Pct Recovery = 90% Analysis Date = 08/04/14 Pct Recovery = 90% Analysis Date = 08/04/14 Pct Recovery = 90% Analysis Date = 07/31/14 Pct Recovery = 90% Analysis Date = 07/31/14 Pct Recovery = 90% Analysis Date = 07/26/14 Pct Recovery = 89% Analysis Date = 07/26/14 Pct Recovery = 89% Analysis Date = 07/21/14 Pct Recovery = 89% Analysis Date = 07/21/14 Pct Recovery = 89% Analysis Date = 07/16/14 Pct Recovery = 89% Analysis Date = 07/16/14 Pct Recovery = 89% Analysis Date = 07/11/14 Pct Recovery = 89% Analysis Date = 07/11/14 Pct Recovery = 89% Analysis Date = 07/07/14 Pct Recovery = 89% Analysis Date = 07/07/14 Pct Recovery = 89% Analysis Date = 07/02/14 Pct Recovery = 89% Analysis Date = 07/02/14 Pct Recovery = 89% Analysis Date = 06/27/14 Pct Recovery = 89% Analysis Date = 06/27/14 Pct Recovery = 89% Analysis Date = 06/22/14 Pct Recovery = 88% Analysis Date = 06/22/14 Pct Recovery = 88% Analysis Date = 06/17/14 Pct Recovery = 88% Analysis Date = 06/17/14 Pct Recovery = 88% Analysis Date = 06/13/14 Pct Recovery = 88% Analysis Date = 06/13/14 Pct Recovery = 88% Analysis Date = 06/08/14 Pct Recovery = 88% Analysis Date = 06/08/14 Pct Recovery = 88% Analysis Date = 06/03/14 Pct Recovery = 88% Analysis Date = 06/03/14 Pct Recovery = 88% Analysis Date = 05/29/14 Pct Recovery = 88% Analysis Date = 05/29/14 Pct Recovery = 88% Analysis Date = 05/24/14 Pct Recovery = 87% Analysis Date = 05/24/14 Pct Recovery = 87% Analysis Date = 05/20/14 Pct Recovery = 87% Analysis Date = 05/20/14 Pct Recovery = 87% Analysis Date = 05/15/14 Pct Recovery = 87% Analysis Date = 05/15/14 Pct Recovery = 87% Analysis Date = 05/10/14 Pct Recovery = 87% Analysis Date = 05/10/14 Pct Recovery = 87% Analysis Date = 05/05/14 Pct Recovery = 87% Analysis Date = 05/05/14 Pct Recovery = 87% Analysis Date = 05/01/14 Pct Recovery = 87% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
O-ETHYL TOLUENE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 51 89% 10% 89% 8%
Total 51 89% 10% 89% 8%

Sample Statistics
O-ETHYL TOLUENE

Characteristic N % % Basis
Plotted 51 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 51 .  
False Negatives 0 0% 0 out of 51
Not Spiked 22 .  
False Positives 0 0% 0 out of 22

BQS OBSP Determination:
O-XYLENE
METHOD: 4440 , TESTIDCODE: 77135GCM66
Open Data Set

Analysis Date = 12/16/16 SpikeMix = NSI 041816AVOC: 40 µl & ChemService 5082900: 40 µl Pct Recovery = 94% Analysis Date = 08/04/16 SpikeMix = Crescent 03FF058: 40 µl & Supelco LC20141V: 40 µl Pct Recovery = 89% Analysis Date = 07/20/16 SpikeMix = Supelco LC20141V: 40 µl & Accu 216041125: 40 µl Pct Recovery = 86% Analysis Date = 11/21/16 SpikeMix = Crescent 03FF058: 25 µl & Supelco LC20141V: 25 µl Pct Recovery = 90% Analysis Date = 09/08/16 SpikeMix = Supelco LC20141V: 25 µl & Accu 216041125: 25 µl Pct Recovery = 85% Analysis Date = 08/26/16 SpikeMix = NSI 041816AVOC: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 87% Analysis Date = 08/12/16 SpikeMix = ChemService 5082900: 25 µl & Phenova B20160319: 25 µl Pct Recovery = 91% Analysis Date = 06/30/16 SpikeMix = Crescent 03FF058: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 93% Analysis Date = 03/19/15 SpikeMix = Spex Organics C1140417015: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 93% Analysis Date = 12/17/14 SpikeMix = Supelco LC06438: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 119% Analysis Date = 11/14/14 SpikeMix = Crescent 03DD004: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 86% Analysis Date = 06/10/14 SpikeMix = Crescent 03DD004: 20 µl & NSI 032614: 20 µl Pct Recovery = 83% Analysis Date = 04/09/15 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 98% Analysis Date = 08/19/14 SpikeMix = Spex Organics C1140417015: 20 µl & Accu 214031115: 20 µl Pct Recovery = 101% Analysis Date = 07/01/14 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 96% Analysis Date = 05/01/14 SpikeMix = Accu 214031115: 20 µl & NSI 032614: 20 µl Pct Recovery = 86% Analysis Date = 08/15/15 SpikeMix = Supelco LC13545: 25 µl & Crescent 04EE008: 25 µl Pct Recovery = 89% Analysis Date = 06/16/15 SpikeMix = ERA 0406-15-03: 25 µl & Supelco LC13545: 25 µl Pct Recovery = 80% Analysis Date = 11/29/16 SpikeMix = ChemService 5082900: 15 µl & Phenova B20160319: 15 µl Pct Recovery = 93% Analysis Date = 10/13/16 SpikeMix = NSI 041816AVOC: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 100% Analysis Date = 09/28/16 SpikeMix = Crescent 03FF058: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 98% Analysis Date = 06/30/16 SpikeMix = ChemService 5082900: 15 µl & Accu 216041125: 15 µl Pct Recovery = 88% Analysis Date = 06/10/16 SpikeMix = NSI 041816AVOC: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 99% Analysis Date = 05/27/16 SpikeMix = Phenova B20160319: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 89% Analysis Date = 04/02/16 SpikeMix = Supelco LC13545: 15 µl & Accu 215041380: 15 µl Pct Recovery = 98% Analysis Date = 12/18/15 SpikeMix = Supelco LC13545: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 92% Analysis Date = 04/26/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 88% Analysis Date = 02/05/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 93% Analysis Date = 11/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 86% Analysis Date = 10/16/15 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 94% Analysis Date = 05/09/15 SpikeMix = Spex Organics EN150428007: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 105% Analysis Date = 11/06/14 SpikeMix = Spex Organics C1140417015: 10 µl & Crescent 03DD004: 10 µl Pct Recovery = 95% Analysis Date = 10/04/14 SpikeMix = Crescent 03DD004: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 88% Analysis Date = 07/29/14 SpikeMix = Crescent 03DD004: 10 µl & NSI 032614: 10 µl Pct Recovery = 97% Analysis Date = 05/03/14 SpikeMix = Crescent 03DD004: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 137% Analysis Date = 01/13/15 SpikeMix = Accu 214031115: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 105% Analysis Date = 09/09/14 SpikeMix = Accu 214031115: 10 µl & NSI 032614: 10 µl Pct Recovery = 128% Analysis Date = 07/23/14 SpikeMix = Spex Organics C1140417015: 10 µl & Accu 214031115: 10 µl Pct Recovery = 113% Analysis Date = 06/18/14 SpikeMix = Supelco LC06438: 10 µl & Accu 214031115: 10 µl Pct Recovery = 91% Analysis Date = 05/13/16 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 97% Analysis Date = 03/17/16 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 76% Analysis Date = 12/10/15 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 94% Analysis Date = 06/27/15 SpikeMix = ERA 0406-15-03: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 100% Analysis Date = 05/09/15 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 106% Analysis Date = 02/18/16 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 99% Analysis Date = 11/12/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 94% Analysis Date = 09/03/15 SpikeMix = NSI 050515AVOC: 10 µl & Spex Organics EN150428007: 10 µl Pct Recovery = 95% Analysis Date = 05/21/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 113% Analysis Date = 12/15/16 Pct Recovery = 92% Analysis Date = 12/11/16 Pct Recovery = 92% Analysis Date = 12/11/16 Pct Recovery = 92% Analysis Date = 12/06/16 Pct Recovery = 92% Analysis Date = 12/06/16 Pct Recovery = 92% Analysis Date = 12/01/16 Pct Recovery = 92% Analysis Date = 12/01/16 Pct Recovery = 92% Analysis Date = 11/26/16 Pct Recovery = 92% Analysis Date = 11/26/16 Pct Recovery = 92% Analysis Date = 11/21/16 Pct Recovery = 92% Analysis Date = 11/21/16 Pct Recovery = 92% Analysis Date = 11/17/16 Pct Recovery = 92% Analysis Date = 11/17/16 Pct Recovery = 92% Analysis Date = 11/12/16 Pct Recovery = 92% Analysis Date = 11/12/16 Pct Recovery = 92% Analysis Date = 11/07/16 Pct Recovery = 92% Analysis Date = 11/07/16 Pct Recovery = 92% Analysis Date = 11/02/16 Pct Recovery = 92% Analysis Date = 11/02/16 Pct Recovery = 92% Analysis Date = 10/28/16 Pct Recovery = 92% Analysis Date = 10/28/16 Pct Recovery = 92% Analysis Date = 10/24/16 Pct Recovery = 92% Analysis Date = 10/24/16 Pct Recovery = 92% Analysis Date = 10/19/16 Pct Recovery = 92% Analysis Date = 10/19/16 Pct Recovery = 92% Analysis Date = 10/14/16 Pct Recovery = 92% Analysis Date = 10/14/16 Pct Recovery = 92% Analysis Date = 10/09/16 Pct Recovery = 92% Analysis Date = 10/09/16 Pct Recovery = 92% Analysis Date = 10/04/16 Pct Recovery = 92% Analysis Date = 10/04/16 Pct Recovery = 92% Analysis Date = 09/30/16 Pct Recovery = 92% Analysis Date = 09/30/16 Pct Recovery = 92% Analysis Date = 09/25/16 Pct Recovery = 92% Analysis Date = 09/25/16 Pct Recovery = 92% Analysis Date = 09/20/16 Pct Recovery = 92% Analysis Date = 09/20/16 Pct Recovery = 92% Analysis Date = 09/15/16 Pct Recovery = 92% Analysis Date = 09/15/16 Pct Recovery = 92% Analysis Date = 09/10/16 Pct Recovery = 92% Analysis Date = 09/10/16 Pct Recovery = 92% Analysis Date = 09/06/16 Pct Recovery = 92% Analysis Date = 09/06/16 Pct Recovery = 92% Analysis Date = 09/01/16 Pct Recovery = 92% Analysis Date = 09/01/16 Pct Recovery = 92% Analysis Date = 08/27/16 Pct Recovery = 92% Analysis Date = 08/27/16 Pct Recovery = 92% Analysis Date = 08/22/16 Pct Recovery = 92% Analysis Date = 08/22/16 Pct Recovery = 92% Analysis Date = 08/17/16 Pct Recovery = 92% Analysis Date = 08/17/16 Pct Recovery = 92% Analysis Date = 08/13/16 Pct Recovery = 92% Analysis Date = 08/13/16 Pct Recovery = 92% Analysis Date = 08/08/16 Pct Recovery = 92% Analysis Date = 08/08/16 Pct Recovery = 92% Analysis Date = 08/03/16 Pct Recovery = 92% Analysis Date = 08/03/16 Pct Recovery = 92% Analysis Date = 07/29/16 Pct Recovery = 92% Analysis Date = 07/29/16 Pct Recovery = 92% Analysis Date = 07/24/16 Pct Recovery = 92% Analysis Date = 07/24/16 Pct Recovery = 92% Analysis Date = 07/20/16 Pct Recovery = 92% Analysis Date = 07/20/16 Pct Recovery = 92% Analysis Date = 07/15/16 Pct Recovery = 92% Analysis Date = 07/15/16 Pct Recovery = 92% Analysis Date = 07/10/16 Pct Recovery = 92% Analysis Date = 07/10/16 Pct Recovery = 92% Analysis Date = 07/05/16 Pct Recovery = 92% Analysis Date = 07/05/16 Pct Recovery = 92% Analysis Date = 06/30/16 Pct Recovery = 92% Analysis Date = 06/30/16 Pct Recovery = 92% Analysis Date = 06/26/16 Pct Recovery = 92% Analysis Date = 06/26/16 Pct Recovery = 92% Analysis Date = 06/21/16 Pct Recovery = 92% Analysis Date = 06/21/16 Pct Recovery = 92% Analysis Date = 06/16/16 Pct Recovery = 92% Analysis Date = 06/16/16 Pct Recovery = 92% Analysis Date = 06/11/16 Pct Recovery = 92% Analysis Date = 06/11/16 Pct Recovery = 92% Analysis Date = 06/06/16 Pct Recovery = 92% Analysis Date = 06/06/16 Pct Recovery = 92% Analysis Date = 06/02/16 Pct Recovery = 92% Analysis Date = 06/02/16 Pct Recovery = 92% Analysis Date = 05/28/16 Pct Recovery = 92% Analysis Date = 05/28/16 Pct Recovery = 92% Analysis Date = 05/23/16 Pct Recovery = 92% Analysis Date = 05/23/16 Pct Recovery = 92% Analysis Date = 05/18/16 Pct Recovery = 92% Analysis Date = 05/18/16 Pct Recovery = 92% Analysis Date = 05/13/16 Pct Recovery = 92% Analysis Date = 05/13/16 Pct Recovery = 92% Analysis Date = 05/09/16 Pct Recovery = 92% Analysis Date = 05/09/16 Pct Recovery = 92% Analysis Date = 05/04/16 Pct Recovery = 92% Analysis Date = 05/04/16 Pct Recovery = 92% Analysis Date = 04/29/16 Pct Recovery = 92% Analysis Date = 04/29/16 Pct Recovery = 92% Analysis Date = 04/24/16 Pct Recovery = 92% Analysis Date = 04/24/16 Pct Recovery = 92% Analysis Date = 04/19/16 Pct Recovery = 92% Analysis Date = 04/19/16 Pct Recovery = 92% Analysis Date = 04/15/16 Pct Recovery = 92% Analysis Date = 04/15/16 Pct Recovery = 92% Analysis Date = 04/10/16 Pct Recovery = 92% Analysis Date = 04/10/16 Pct Recovery = 92% Analysis Date = 04/05/16 Pct Recovery = 92% Analysis Date = 04/05/16 Pct Recovery = 92% Analysis Date = 03/31/16 Pct Recovery = 92% Analysis Date = 03/31/16 Pct Recovery = 92% Analysis Date = 03/26/16 Pct Recovery = 92% Analysis Date = 03/26/16 Pct Recovery = 92% Analysis Date = 03/22/16 Pct Recovery = 92% Analysis Date = 03/22/16 Pct Recovery = 92% Analysis Date = 03/17/16 Pct Recovery = 92% Analysis Date = 03/17/16 Pct Recovery = 92% Analysis Date = 03/12/16 Pct Recovery = 92% Analysis Date = 03/12/16 Pct Recovery = 92% Analysis Date = 03/07/16 Pct Recovery = 92% Analysis Date = 03/07/16 Pct Recovery = 92% Analysis Date = 03/02/16 Pct Recovery = 92% Analysis Date = 03/02/16 Pct Recovery = 92% Analysis Date = 02/27/16 Pct Recovery = 92% Analysis Date = 02/27/16 Pct Recovery = 92% Analysis Date = 02/22/16 Pct Recovery = 92% Analysis Date = 02/22/16 Pct Recovery = 92% Analysis Date = 02/17/16 Pct Recovery = 92% Analysis Date = 02/17/16 Pct Recovery = 92% Analysis Date = 02/12/16 Pct Recovery = 92% Analysis Date = 02/12/16 Pct Recovery = 92% Analysis Date = 02/07/16 Pct Recovery = 92% Analysis Date = 02/07/16 Pct Recovery = 92% Analysis Date = 02/03/16 Pct Recovery = 92% Analysis Date = 02/03/16 Pct Recovery = 92% Analysis Date = 01/29/16 Pct Recovery = 92% Analysis Date = 01/29/16 Pct Recovery = 92% Analysis Date = 01/24/16 Pct Recovery = 92% Analysis Date = 01/24/16 Pct Recovery = 92% Analysis Date = 01/19/16 Pct Recovery = 92% Analysis Date = 01/19/16 Pct Recovery = 92% Analysis Date = 01/14/16 Pct Recovery = 92% Analysis Date = 01/14/16 Pct Recovery = 92% Analysis Date = 01/10/16 Pct Recovery = 92% Analysis Date = 01/10/16 Pct Recovery = 92% Analysis Date = 01/05/16 Pct Recovery = 92% Analysis Date = 01/05/16 Pct Recovery = 92% Analysis Date = 12/31/15 Pct Recovery = 92% Analysis Date = 12/31/15 Pct Recovery = 92% Analysis Date = 12/26/15 Pct Recovery = 92% Analysis Date = 12/26/15 Pct Recovery = 92% Analysis Date = 12/21/15 Pct Recovery = 92% Analysis Date = 12/21/15 Pct Recovery = 92% Analysis Date = 12/17/15 Pct Recovery = 92% Analysis Date = 12/17/15 Pct Recovery = 92% Analysis Date = 12/12/15 Pct Recovery = 92% Analysis Date = 12/12/15 Pct Recovery = 92% Analysis Date = 12/07/15 Pct Recovery = 92% Analysis Date = 12/07/15 Pct Recovery = 92% Analysis Date = 12/02/15 Pct Recovery = 93% Analysis Date = 12/02/15 Pct Recovery = 93% Analysis Date = 11/27/15 Pct Recovery = 93% Analysis Date = 11/27/15 Pct Recovery = 93% Analysis Date = 11/23/15 Pct Recovery = 93% Analysis Date = 11/23/15 Pct Recovery = 93% Analysis Date = 11/18/15 Pct Recovery = 93% Analysis Date = 11/18/15 Pct Recovery = 93% Analysis Date = 11/13/15 Pct Recovery = 93% Analysis Date = 11/13/15 Pct Recovery = 93% Analysis Date = 11/08/15 Pct Recovery = 93% Analysis Date = 11/08/15 Pct Recovery = 93% Analysis Date = 11/03/15 Pct Recovery = 93% Analysis Date = 11/03/15 Pct Recovery = 93% Analysis Date = 10/30/15 Pct Recovery = 94% Analysis Date = 10/30/15 Pct Recovery = 94% Analysis Date = 10/25/15 Pct Recovery = 94% Analysis Date = 10/25/15 Pct Recovery = 94% Analysis Date = 10/20/15 Pct Recovery = 94% Analysis Date = 10/20/15 Pct Recovery = 94% Analysis Date = 10/15/15 Pct Recovery = 94% Analysis Date = 10/15/15 Pct Recovery = 94% Analysis Date = 10/10/15 Pct Recovery = 94% Analysis Date = 10/10/15 Pct Recovery = 94% Analysis Date = 10/06/15 Pct Recovery = 94% Analysis Date = 10/06/15 Pct Recovery = 94% Analysis Date = 10/01/15 Pct Recovery = 94% Analysis Date = 10/01/15 Pct Recovery = 94% Analysis Date = 09/26/15 Pct Recovery = 94% Analysis Date = 09/26/15 Pct Recovery = 94% Analysis Date = 09/21/15 Pct Recovery = 95% Analysis Date = 09/21/15 Pct Recovery = 95% Analysis Date = 09/16/15 Pct Recovery = 95% Analysis Date = 09/16/15 Pct Recovery = 95% Analysis Date = 09/12/15 Pct Recovery = 95% Analysis Date = 09/12/15 Pct Recovery = 95% Analysis Date = 09/07/15 Pct Recovery = 95% Analysis Date = 09/07/15 Pct Recovery = 95% Analysis Date = 09/02/15 Pct Recovery = 95% Analysis Date = 09/02/15 Pct Recovery = 95% Analysis Date = 08/28/15 Pct Recovery = 95% Analysis Date = 08/28/15 Pct Recovery = 95% Analysis Date = 08/23/15 Pct Recovery = 95% Analysis Date = 08/23/15 Pct Recovery = 95% Analysis Date = 08/19/15 Pct Recovery = 95% Analysis Date = 08/19/15 Pct Recovery = 95% Analysis Date = 08/14/15 Pct Recovery = 96% Analysis Date = 08/14/15 Pct Recovery = 96% Analysis Date = 08/09/15 Pct Recovery = 96% Analysis Date = 08/09/15 Pct Recovery = 96% Analysis Date = 08/04/15 Pct Recovery = 96% Analysis Date = 08/04/15 Pct Recovery = 96% Analysis Date = 07/30/15 Pct Recovery = 96% Analysis Date = 07/30/15 Pct Recovery = 96% Analysis Date = 07/26/15 Pct Recovery = 96% Analysis Date = 07/26/15 Pct Recovery = 96% Analysis Date = 07/21/15 Pct Recovery = 96% Analysis Date = 07/21/15 Pct Recovery = 96% Analysis Date = 07/16/15 Pct Recovery = 96% Analysis Date = 07/16/15 Pct Recovery = 96% Analysis Date = 07/11/15 Pct Recovery = 97% Analysis Date = 07/11/15 Pct Recovery = 97% Analysis Date = 07/06/15 Pct Recovery = 97% Analysis Date = 07/06/15 Pct Recovery = 97% Analysis Date = 07/02/15 Pct Recovery = 97% Analysis Date = 07/02/15 Pct Recovery = 97% Analysis Date = 06/27/15 Pct Recovery = 97% Analysis Date = 06/27/15 Pct Recovery = 97% Analysis Date = 06/22/15 Pct Recovery = 97% Analysis Date = 06/22/15 Pct Recovery = 97% Analysis Date = 06/17/15 Pct Recovery = 97% Analysis Date = 06/17/15 Pct Recovery = 97% Analysis Date = 06/12/15 Pct Recovery = 97% Analysis Date = 06/12/15 Pct Recovery = 97% Analysis Date = 06/08/15 Pct Recovery = 97% Analysis Date = 06/08/15 Pct Recovery = 97% Analysis Date = 06/03/15 Pct Recovery = 97% Analysis Date = 06/03/15 Pct Recovery = 97% Analysis Date = 05/29/15 Pct Recovery = 98% Analysis Date = 05/29/15 Pct Recovery = 98% Analysis Date = 05/24/15 Pct Recovery = 98% Analysis Date = 05/24/15 Pct Recovery = 98% Analysis Date = 05/19/15 Pct Recovery = 98% Analysis Date = 05/19/15 Pct Recovery = 98% Analysis Date = 05/15/15 Pct Recovery = 98% Analysis Date = 05/15/15 Pct Recovery = 98% Analysis Date = 05/10/15 Pct Recovery = 98% Analysis Date = 05/10/15 Pct Recovery = 98% Analysis Date = 05/05/15 Pct Recovery = 98% Analysis Date = 05/05/15 Pct Recovery = 98% Analysis Date = 04/30/15 Pct Recovery = 98% Analysis Date = 04/30/15 Pct Recovery = 98% Analysis Date = 04/25/15 Pct Recovery = 98% Analysis Date = 04/25/15 Pct Recovery = 98% Analysis Date = 04/21/15 Pct Recovery = 99% Analysis Date = 04/21/15 Pct Recovery = 99% Analysis Date = 04/16/15 Pct Recovery = 99% Analysis Date = 04/16/15 Pct Recovery = 99% Analysis Date = 04/11/15 Pct Recovery = 99% Analysis Date = 04/11/15 Pct Recovery = 99% Analysis Date = 04/06/15 Pct Recovery = 99% Analysis Date = 04/06/15 Pct Recovery = 99% Analysis Date = 04/01/15 Pct Recovery = 99% Analysis Date = 04/01/15 Pct Recovery = 99% Analysis Date = 03/28/15 Pct Recovery = 99% Analysis Date = 03/28/15 Pct Recovery = 99% Analysis Date = 03/23/15 Pct Recovery = 99% Analysis Date = 03/23/15 Pct Recovery = 99% Analysis Date = 03/18/15 Pct Recovery = 99% Analysis Date = 03/18/15 Pct Recovery = 99% Analysis Date = 03/13/15 Pct Recovery = 99% Analysis Date = 03/13/15 Pct Recovery = 99% Analysis Date = 03/08/15 Pct Recovery = 99% Analysis Date = 03/08/15 Pct Recovery = 99% Analysis Date = 03/04/15 Pct Recovery = 99% Analysis Date = 03/04/15 Pct Recovery = 99% Analysis Date = 02/27/15 Pct Recovery = 100% Analysis Date = 02/27/15 Pct Recovery = 100% Analysis Date = 02/22/15 Pct Recovery = 100% Analysis Date = 02/22/15 Pct Recovery = 100% Analysis Date = 02/17/15 Pct Recovery = 100% Analysis Date = 02/17/15 Pct Recovery = 100% Analysis Date = 02/12/15 Pct Recovery = 100% Analysis Date = 02/12/15 Pct Recovery = 100% Analysis Date = 02/08/15 Pct Recovery = 100% Analysis Date = 02/08/15 Pct Recovery = 100% Analysis Date = 02/03/15 Pct Recovery = 100% Analysis Date = 02/03/15 Pct Recovery = 100% Analysis Date = 01/29/15 Pct Recovery = 100% Analysis Date = 01/29/15 Pct Recovery = 100% Analysis Date = 01/24/15 Pct Recovery = 100% Analysis Date = 01/24/15 Pct Recovery = 100% Analysis Date = 01/19/15 Pct Recovery = 100% Analysis Date = 01/19/15 Pct Recovery = 100% Analysis Date = 01/15/15 Pct Recovery = 100% Analysis Date = 01/15/15 Pct Recovery = 100% Analysis Date = 01/10/15 Pct Recovery = 100% Analysis Date = 01/10/15 Pct Recovery = 100% Analysis Date = 01/05/15 Pct Recovery = 100% Analysis Date = 01/05/15 Pct Recovery = 100% Analysis Date = 12/31/14 Pct Recovery = 100% Analysis Date = 12/31/14 Pct Recovery = 100% Analysis Date = 12/26/14 Pct Recovery = 100% Analysis Date = 12/26/14 Pct Recovery = 100% Analysis Date = 12/22/14 Pct Recovery = 100% Analysis Date = 12/22/14 Pct Recovery = 100% Analysis Date = 12/17/14 Pct Recovery = 100% Analysis Date = 12/17/14 Pct Recovery = 100% Analysis Date = 12/12/14 Pct Recovery = 100% Analysis Date = 12/12/14 Pct Recovery = 100% Analysis Date = 12/07/14 Pct Recovery = 101% Analysis Date = 12/07/14 Pct Recovery = 101% Analysis Date = 12/02/14 Pct Recovery = 101% Analysis Date = 12/02/14 Pct Recovery = 101% Analysis Date = 11/28/14 Pct Recovery = 101% Analysis Date = 11/28/14 Pct Recovery = 101% Analysis Date = 11/23/14 Pct Recovery = 101% Analysis Date = 11/23/14 Pct Recovery = 101% Analysis Date = 11/18/14 Pct Recovery = 101% Analysis Date = 11/18/14 Pct Recovery = 101% Analysis Date = 11/13/14 Pct Recovery = 101% Analysis Date = 11/13/14 Pct Recovery = 101% Analysis Date = 11/08/14 Pct Recovery = 101% Analysis Date = 11/08/14 Pct Recovery = 101% Analysis Date = 11/04/14 Pct Recovery = 101% Analysis Date = 11/04/14 Pct Recovery = 101% Analysis Date = 10/30/14 Pct Recovery = 101% Analysis Date = 10/30/14 Pct Recovery = 101% Analysis Date = 10/25/14 Pct Recovery = 101% Analysis Date = 10/25/14 Pct Recovery = 101% Analysis Date = 10/20/14 Pct Recovery = 101% Analysis Date = 10/20/14 Pct Recovery = 101% Analysis Date = 10/15/14 Pct Recovery = 101% Analysis Date = 10/15/14 Pct Recovery = 101% Analysis Date = 10/11/14 Pct Recovery = 101% Analysis Date = 10/11/14 Pct Recovery = 101% Analysis Date = 10/06/14 Pct Recovery = 101% Analysis Date = 10/06/14 Pct Recovery = 101% Analysis Date = 10/01/14 Pct Recovery = 101% Analysis Date = 10/01/14 Pct Recovery = 101% Analysis Date = 09/26/14 Pct Recovery = 101% Analysis Date = 09/26/14 Pct Recovery = 101% Analysis Date = 09/21/14 Pct Recovery = 101% Analysis Date = 09/21/14 Pct Recovery = 101% Analysis Date = 09/17/14 Pct Recovery = 101% Analysis Date = 09/17/14 Pct Recovery = 101% Analysis Date = 09/12/14 Pct Recovery = 101% Analysis Date = 09/12/14 Pct Recovery = 101% Analysis Date = 09/07/14 Pct Recovery = 101% Analysis Date = 09/07/14 Pct Recovery = 101% Analysis Date = 09/02/14 Pct Recovery = 101% Analysis Date = 09/02/14 Pct Recovery = 101% Analysis Date = 08/28/14 Pct Recovery = 101% Analysis Date = 08/28/14 Pct Recovery = 101% Analysis Date = 08/24/14 Pct Recovery = 101% Analysis Date = 08/24/14 Pct Recovery = 101% Analysis Date = 08/19/14 Pct Recovery = 102% Analysis Date = 08/19/14 Pct Recovery = 102% Analysis Date = 08/14/14 Pct Recovery = 102% Analysis Date = 08/14/14 Pct Recovery = 102% Analysis Date = 08/09/14 Pct Recovery = 102% Analysis Date = 08/09/14 Pct Recovery = 102% Analysis Date = 08/04/14 Pct Recovery = 102% Analysis Date = 08/04/14 Pct Recovery = 102% Analysis Date = 07/31/14 Pct Recovery = 102% Analysis Date = 07/31/14 Pct Recovery = 102% Analysis Date = 07/26/14 Pct Recovery = 102% Analysis Date = 07/26/14 Pct Recovery = 102% Analysis Date = 07/21/14 Pct Recovery = 102% Analysis Date = 07/21/14 Pct Recovery = 102% Analysis Date = 07/16/14 Pct Recovery = 102% Analysis Date = 07/16/14 Pct Recovery = 102% Analysis Date = 07/11/14 Pct Recovery = 102% Analysis Date = 07/11/14 Pct Recovery = 102% Analysis Date = 07/07/14 Pct Recovery = 102% Analysis Date = 07/07/14 Pct Recovery = 102% Analysis Date = 07/02/14 Pct Recovery = 102% Analysis Date = 07/02/14 Pct Recovery = 102% Analysis Date = 06/27/14 Pct Recovery = 102% Analysis Date = 06/27/14 Pct Recovery = 102% Analysis Date = 06/22/14 Pct Recovery = 102% Analysis Date = 06/22/14 Pct Recovery = 102% Analysis Date = 06/17/14 Pct Recovery = 102% Analysis Date = 06/17/14 Pct Recovery = 102% Analysis Date = 06/13/14 Pct Recovery = 102% Analysis Date = 06/13/14 Pct Recovery = 102% Analysis Date = 06/08/14 Pct Recovery = 102% Analysis Date = 06/08/14 Pct Recovery = 102% Analysis Date = 06/03/14 Pct Recovery = 102% Analysis Date = 06/03/14 Pct Recovery = 102% Analysis Date = 05/29/14 Pct Recovery = 102% Analysis Date = 05/29/14 Pct Recovery = 102% Analysis Date = 05/24/14 Pct Recovery = 102% Analysis Date = 05/24/14 Pct Recovery = 102% Analysis Date = 05/20/14 Pct Recovery = 102% Analysis Date = 05/20/14 Pct Recovery = 102% Analysis Date = 05/15/14 Pct Recovery = 102% Analysis Date = 05/15/14 Pct Recovery = 102% Analysis Date = 05/10/14 Pct Recovery = 102% Analysis Date = 05/10/14 Pct Recovery = 102% Analysis Date = 05/05/14 Pct Recovery = 102% Analysis Date = 05/05/14 Pct Recovery = 102% Analysis Date = 05/01/14 Pct Recovery = 102% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
O-XYLENE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 48 96% 11% 94% 8%
Total 48 96% 11% 94% 8%

Sample Statistics
O-XYLENE

Characteristic N % % Basis
Plotted 48 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 48 .  
False Negatives 0 0% 0 out of 48
Not Spiked 25 .  
False Positives 0 0% 0 out of 25

BQS OBSP Determination:
SEC-BUTYLBENZENE
METHOD: 4440 , TESTIDCODE: 77350GCM66
Open Data Set

Analysis Date = 12/16/16 SpikeMix = NSI 041816AVOC: 40 µl & ChemService 5082900: 40 µl Pct Recovery = 96% Analysis Date = 12/12/16 SpikeMix = Accu 216041125: 40 µl & Crescent 03FF058: 40 µl Pct Recovery = 98% Analysis Date = 08/04/16 SpikeMix = Crescent 03FF058: 40 µl & Supelco LC20141V: 40 µl Pct Recovery = 76% Analysis Date = 07/14/16 SpikeMix = Accu 216041125: 40 µl & NSI 041816AVOC: 40 µl Pct Recovery = 116% Analysis Date = 11/21/16 SpikeMix = Crescent 03FF058: 25 µl & Supelco LC20141V: 25 µl Pct Recovery = 79% Analysis Date = 08/26/16 SpikeMix = NSI 041816AVOC: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 89% Analysis Date = 06/30/16 SpikeMix = Crescent 03FF058: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 76% Analysis Date = 06/21/16 SpikeMix = Phenova B20160319: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 96% Analysis Date = 05/24/16 SpikeMix = Accu 216041125: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 89% Analysis Date = 03/19/15 SpikeMix = Spex Organics C1140417015: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 101% Analysis Date = 03/06/15 SpikeMix = ERA 0227-14-06.1A: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 78% Analysis Date = 12/17/14 SpikeMix = Supelco LC06438: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 83% Analysis Date = 11/22/14 SpikeMix = NSI 032614: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 89% Analysis Date = 09/21/14 SpikeMix = Supelco LC06438: 20 µl Pct Recovery = 73% Analysis Date = 08/19/14 SpikeMix = Spex Organics C1140417015: 20 µl & Accu 214031115: 20 µl Pct Recovery = 90% Analysis Date = 08/16/14 SpikeMix = ERA 0227-14-06.1A: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 86% Analysis Date = 06/10/14 SpikeMix = NSI 032614: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 82% Analysis Date = 08/15/15 SpikeMix = Supelco LC13545: 25 µl & Crescent 04EE008: 25 µl Pct Recovery = 97% Analysis Date = 06/16/15 SpikeMix = ERA 0406-15-03: 25 µl & Supelco LC13545: 25 µl Pct Recovery = 83% Analysis Date = 10/13/16 SpikeMix = Accu 216041125: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 114% Analysis Date = 10/13/16 SpikeMix = NSI 041816AVOC: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 97% Analysis Date = 09/28/16 SpikeMix = Crescent 03FF058: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 76% Analysis Date = 09/08/16 SpikeMix = Phenova B20160319: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 81% Analysis Date = 08/20/16 SpikeMix = Accu 216041125: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 90% Analysis Date = 07/29/16 SpikeMix = Phenova B20160319: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 116% Analysis Date = 06/10/16 SpikeMix = NSI 041816AVOC: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 107% Analysis Date = 04/26/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 80% Analysis Date = 02/05/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 88% Analysis Date = 11/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 91% Analysis Date = 10/16/15 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 87% Analysis Date = 05/09/15 SpikeMix = Spex Organics EN150428007: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 90% Analysis Date = 04/02/16 SpikeMix = Supelco LC13545: 15 µl & Accu 215041380: 15 µl Pct Recovery = 89% Analysis Date = 12/18/15 SpikeMix = Supelco LC13545: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 88% Analysis Date = 11/06/14 SpikeMix = Spex Organics C1140417015: 10 µl & Crescent 03DD004: 10 µl Pct Recovery = 101% Analysis Date = 10/21/14 SpikeMix = ERA 0227-14-06.1A: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 80% Analysis Date = 09/09/14 SpikeMix = NSI 032614: 10 µl & Spex Organics C1140417015: 10 µl Pct Recovery = 98% Analysis Date = 07/23/14 SpikeMix = Spex Organics C1140417015: 10 µl & Accu 214031115: 10 µl Pct Recovery = 100% Analysis Date = 07/11/14 SpikeMix = Spex Organics C1140417015: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 92% Analysis Date = 06/18/14 SpikeMix = Supelco LC06438: 10 µl & Accu 214031115: 10 µl Pct Recovery = 81% Analysis Date = 05/30/14 SpikeMix = NSI 032614: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 71% Analysis Date = 05/03/14 SpikeMix = Crescent 03DD004: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 94% Analysis Date = 02/18/16 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 91% Analysis Date = 11/12/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 100% Analysis Date = 09/03/15 SpikeMix = NSI 050515AVOC: 10 µl & Spex Organics EN150428007: 10 µl Pct Recovery = 79% Analysis Date = 05/21/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 104% Analysis Date = 05/13/16 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 97% Analysis Date = 03/17/16 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 73% Analysis Date = 12/10/15 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 93% Analysis Date = 06/27/15 SpikeMix = ERA 0406-15-03: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 98% Analysis Date = 05/09/15 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 95% Analysis Date = 12/16/16 Pct Recovery = 94% Analysis Date = 12/11/16 Pct Recovery = 94% Analysis Date = 12/11/16 Pct Recovery = 94% Analysis Date = 12/06/16 Pct Recovery = 94% Analysis Date = 12/06/16 Pct Recovery = 94% Analysis Date = 12/01/16 Pct Recovery = 94% Analysis Date = 12/01/16 Pct Recovery = 94% Analysis Date = 11/26/16 Pct Recovery = 94% Analysis Date = 11/26/16 Pct Recovery = 94% Analysis Date = 11/22/16 Pct Recovery = 94% Analysis Date = 11/22/16 Pct Recovery = 94% Analysis Date = 11/17/16 Pct Recovery = 94% Analysis Date = 11/17/16 Pct Recovery = 94% Analysis Date = 11/12/16 Pct Recovery = 94% Analysis Date = 11/12/16 Pct Recovery = 94% Analysis Date = 11/07/16 Pct Recovery = 94% Analysis Date = 11/07/16 Pct Recovery = 94% Analysis Date = 11/02/16 Pct Recovery = 93% Analysis Date = 11/02/16 Pct Recovery = 93% Analysis Date = 10/29/16 Pct Recovery = 93% Analysis Date = 10/29/16 Pct Recovery = 93% Analysis Date = 10/24/16 Pct Recovery = 93% Analysis Date = 10/24/16 Pct Recovery = 93% Analysis Date = 10/19/16 Pct Recovery = 93% Analysis Date = 10/19/16 Pct Recovery = 93% Analysis Date = 10/14/16 Pct Recovery = 93% Analysis Date = 10/14/16 Pct Recovery = 93% Analysis Date = 10/09/16 Pct Recovery = 93% Analysis Date = 10/09/16 Pct Recovery = 93% Analysis Date = 10/05/16 Pct Recovery = 93% Analysis Date = 10/05/16 Pct Recovery = 93% Analysis Date = 09/30/16 Pct Recovery = 93% Analysis Date = 09/30/16 Pct Recovery = 93% Analysis Date = 09/25/16 Pct Recovery = 93% Analysis Date = 09/25/16 Pct Recovery = 93% Analysis Date = 09/20/16 Pct Recovery = 93% Analysis Date = 09/20/16 Pct Recovery = 93% Analysis Date = 09/15/16 Pct Recovery = 93% Analysis Date = 09/15/16 Pct Recovery = 93% Analysis Date = 09/11/16 Pct Recovery = 93% Analysis Date = 09/11/16 Pct Recovery = 93% Analysis Date = 09/06/16 Pct Recovery = 93% Analysis Date = 09/06/16 Pct Recovery = 93% Analysis Date = 09/01/16 Pct Recovery = 93% Analysis Date = 09/01/16 Pct Recovery = 93% Analysis Date = 08/27/16 Pct Recovery = 93% Analysis Date = 08/27/16 Pct Recovery = 93% Analysis Date = 08/23/16 Pct Recovery = 92% Analysis Date = 08/23/16 Pct Recovery = 92% Analysis Date = 08/18/16 Pct Recovery = 92% Analysis Date = 08/18/16 Pct Recovery = 92% Analysis Date = 08/13/16 Pct Recovery = 92% Analysis Date = 08/13/16 Pct Recovery = 92% Analysis Date = 08/08/16 Pct Recovery = 92% Analysis Date = 08/08/16 Pct Recovery = 92% Analysis Date = 08/03/16 Pct Recovery = 92% Analysis Date = 08/03/16 Pct Recovery = 92% Analysis Date = 07/30/16 Pct Recovery = 92% Analysis Date = 07/30/16 Pct Recovery = 92% Analysis Date = 07/25/16 Pct Recovery = 92% Analysis Date = 07/25/16 Pct Recovery = 92% Analysis Date = 07/20/16 Pct Recovery = 92% Analysis Date = 07/20/16 Pct Recovery = 92% Analysis Date = 07/15/16 Pct Recovery = 92% Analysis Date = 07/15/16 Pct Recovery = 92% Analysis Date = 07/10/16 Pct Recovery = 92% Analysis Date = 07/10/16 Pct Recovery = 92% Analysis Date = 07/06/16 Pct Recovery = 92% Analysis Date = 07/06/16 Pct Recovery = 92% Analysis Date = 07/01/16 Pct Recovery = 92% Analysis Date = 07/01/16 Pct Recovery = 92% Analysis Date = 06/26/16 Pct Recovery = 92% Analysis Date = 06/26/16 Pct Recovery = 92% Analysis Date = 06/21/16 Pct Recovery = 92% Analysis Date = 06/21/16 Pct Recovery = 92% Analysis Date = 06/16/16 Pct Recovery = 92% Analysis Date = 06/16/16 Pct Recovery = 92% Analysis Date = 06/12/16 Pct Recovery = 92% Analysis Date = 06/12/16 Pct Recovery = 92% Analysis Date = 06/07/16 Pct Recovery = 91% Analysis Date = 06/07/16 Pct Recovery = 91% Analysis Date = 06/02/16 Pct Recovery = 91% Analysis Date = 06/02/16 Pct Recovery = 91% Analysis Date = 05/28/16 Pct Recovery = 91% Analysis Date = 05/28/16 Pct Recovery = 91% Analysis Date = 05/24/16 Pct Recovery = 91% Analysis Date = 05/24/16 Pct Recovery = 91% Analysis Date = 05/19/16 Pct Recovery = 91% Analysis Date = 05/19/16 Pct Recovery = 91% Analysis Date = 05/14/16 Pct Recovery = 91% Analysis Date = 05/14/16 Pct Recovery = 91% Analysis Date = 05/09/16 Pct Recovery = 91% Analysis Date = 05/09/16 Pct Recovery = 91% Analysis Date = 05/04/16 Pct Recovery = 91% Analysis Date = 05/04/16 Pct Recovery = 91% Analysis Date = 04/30/16 Pct Recovery = 91% Analysis Date = 04/30/16 Pct Recovery = 91% Analysis Date = 04/25/16 Pct Recovery = 91% Analysis Date = 04/25/16 Pct Recovery = 91% Analysis Date = 04/20/16 Pct Recovery = 91% Analysis Date = 04/20/16 Pct Recovery = 91% Analysis Date = 04/15/16 Pct Recovery = 91% Analysis Date = 04/15/16 Pct Recovery = 91% Analysis Date = 04/10/16 Pct Recovery = 91% Analysis Date = 04/10/16 Pct Recovery = 91% Analysis Date = 04/06/16 Pct Recovery = 91% Analysis Date = 04/06/16 Pct Recovery = 91% Analysis Date = 04/01/16 Pct Recovery = 91% Analysis Date = 04/01/16 Pct Recovery = 91% Analysis Date = 03/27/16 Pct Recovery = 91% Analysis Date = 03/27/16 Pct Recovery = 91% Analysis Date = 03/22/16 Pct Recovery = 91% Analysis Date = 03/22/16 Pct Recovery = 91% Analysis Date = 03/17/16 Pct Recovery = 91% Analysis Date = 03/17/16 Pct Recovery = 91% Analysis Date = 03/13/16 Pct Recovery = 91% Analysis Date = 03/13/16 Pct Recovery = 91% Analysis Date = 03/08/16 Pct Recovery = 91% Analysis Date = 03/08/16 Pct Recovery = 91% Analysis Date = 03/03/16 Pct Recovery = 90% Analysis Date = 03/03/16 Pct Recovery = 90% Analysis Date = 02/27/16 Pct Recovery = 90% Analysis Date = 02/27/16 Pct Recovery = 90% Analysis Date = 02/23/16 Pct Recovery = 90% Analysis Date = 02/23/16 Pct Recovery = 90% Analysis Date = 02/18/16 Pct Recovery = 90% Analysis Date = 02/18/16 Pct Recovery = 90% Analysis Date = 02/13/16 Pct Recovery = 90% Analysis Date = 02/13/16 Pct Recovery = 90% Analysis Date = 02/08/16 Pct Recovery = 90% Analysis Date = 02/08/16 Pct Recovery = 90% Analysis Date = 02/03/16 Pct Recovery = 90% Analysis Date = 02/03/16 Pct Recovery = 90% Analysis Date = 01/30/16 Pct Recovery = 90% Analysis Date = 01/30/16 Pct Recovery = 90% Analysis Date = 01/25/16 Pct Recovery = 90% Analysis Date = 01/25/16 Pct Recovery = 90% Analysis Date = 01/20/16 Pct Recovery = 90% Analysis Date = 01/20/16 Pct Recovery = 90% Analysis Date = 01/15/16 Pct Recovery = 90% Analysis Date = 01/15/16 Pct Recovery = 90% Analysis Date = 01/10/16 Pct Recovery = 90% Analysis Date = 01/10/16 Pct Recovery = 90% Analysis Date = 01/06/16 Pct Recovery = 90% Analysis Date = 01/06/16 Pct Recovery = 90% Analysis Date = 01/01/16 Pct Recovery = 90% Analysis Date = 01/01/16 Pct Recovery = 90% Analysis Date = 12/27/15 Pct Recovery = 90% Analysis Date = 12/27/15 Pct Recovery = 90% Analysis Date = 12/22/15 Pct Recovery = 90% Analysis Date = 12/22/15 Pct Recovery = 90% Analysis Date = 12/17/15 Pct Recovery = 90% Analysis Date = 12/17/15 Pct Recovery = 90% Analysis Date = 12/13/15 Pct Recovery = 90% Analysis Date = 12/13/15 Pct Recovery = 90% Analysis Date = 12/08/15 Pct Recovery = 90% Analysis Date = 12/08/15 Pct Recovery = 90% Analysis Date = 12/03/15 Pct Recovery = 90% Analysis Date = 12/03/15 Pct Recovery = 90% Analysis Date = 11/28/15 Pct Recovery = 90% Analysis Date = 11/28/15 Pct Recovery = 90% Analysis Date = 11/24/15 Pct Recovery = 90% Analysis Date = 11/24/15 Pct Recovery = 90% Analysis Date = 11/19/15 Pct Recovery = 90% Analysis Date = 11/19/15 Pct Recovery = 90% Analysis Date = 11/14/15 Pct Recovery = 90% Analysis Date = 11/14/15 Pct Recovery = 90% Analysis Date = 11/09/15 Pct Recovery = 90% Analysis Date = 11/09/15 Pct Recovery = 90% Analysis Date = 11/04/15 Pct Recovery = 90% Analysis Date = 11/04/15 Pct Recovery = 90% Analysis Date = 10/31/15 Pct Recovery = 91% Analysis Date = 10/31/15 Pct Recovery = 91% Analysis Date = 10/26/15 Pct Recovery = 91% Analysis Date = 10/26/15 Pct Recovery = 91% Analysis Date = 10/21/15 Pct Recovery = 91% Analysis Date = 10/21/15 Pct Recovery = 91% Analysis Date = 10/16/15 Pct Recovery = 91% Analysis Date = 10/16/15 Pct Recovery = 91% Analysis Date = 10/11/15 Pct Recovery = 91% Analysis Date = 10/11/15 Pct Recovery = 91% Analysis Date = 10/07/15 Pct Recovery = 91% Analysis Date = 10/07/15 Pct Recovery = 91% Analysis Date = 10/02/15 Pct Recovery = 91% Analysis Date = 10/02/15 Pct Recovery = 91% Analysis Date = 09/27/15 Pct Recovery = 91% Analysis Date = 09/27/15 Pct Recovery = 91% Analysis Date = 09/22/15 Pct Recovery = 91% Analysis Date = 09/22/15 Pct Recovery = 91% Analysis Date = 09/17/15 Pct Recovery = 91% Analysis Date = 09/17/15 Pct Recovery = 91% Analysis Date = 09/13/15 Pct Recovery = 91% Analysis Date = 09/13/15 Pct Recovery = 91% Analysis Date = 09/08/15 Pct Recovery = 91% Analysis Date = 09/08/15 Pct Recovery = 91% Analysis Date = 09/03/15 Pct Recovery = 91% Analysis Date = 09/03/15 Pct Recovery = 91% Analysis Date = 08/29/15 Pct Recovery = 91% Analysis Date = 08/29/15 Pct Recovery = 91% Analysis Date = 08/25/15 Pct Recovery = 91% Analysis Date = 08/25/15 Pct Recovery = 91% Analysis Date = 08/20/15 Pct Recovery = 91% Analysis Date = 08/20/15 Pct Recovery = 91% Analysis Date = 08/15/15 Pct Recovery = 91% Analysis Date = 08/15/15 Pct Recovery = 91% Analysis Date = 08/10/15 Pct Recovery = 91% Analysis Date = 08/10/15 Pct Recovery = 91% Analysis Date = 08/05/15 Pct Recovery = 91% Analysis Date = 08/05/15 Pct Recovery = 91% Analysis Date = 08/01/15 Pct Recovery = 91% Analysis Date = 08/01/15 Pct Recovery = 91% Analysis Date = 07/27/15 Pct Recovery = 91% Analysis Date = 07/27/15 Pct Recovery = 91% Analysis Date = 07/22/15 Pct Recovery = 91% Analysis Date = 07/22/15 Pct Recovery = 91% Analysis Date = 07/17/15 Pct Recovery = 91% Analysis Date = 07/17/15 Pct Recovery = 91% Analysis Date = 07/12/15 Pct Recovery = 91% Analysis Date = 07/12/15 Pct Recovery = 91% Analysis Date = 07/08/15 Pct Recovery = 91% Analysis Date = 07/08/15 Pct Recovery = 91% Analysis Date = 07/03/15 Pct Recovery = 91% Analysis Date = 07/03/15 Pct Recovery = 91% Analysis Date = 06/28/15 Pct Recovery = 91% Analysis Date = 06/28/15 Pct Recovery = 91% Analysis Date = 06/23/15 Pct Recovery = 91% Analysis Date = 06/23/15 Pct Recovery = 91% Analysis Date = 06/18/15 Pct Recovery = 91% Analysis Date = 06/18/15 Pct Recovery = 91% Analysis Date = 06/14/15 Pct Recovery = 91% Analysis Date = 06/14/15 Pct Recovery = 91% Analysis Date = 06/09/15 Pct Recovery = 91% Analysis Date = 06/09/15 Pct Recovery = 91% Analysis Date = 06/04/15 Pct Recovery = 91% Analysis Date = 06/04/15 Pct Recovery = 91% Analysis Date = 05/30/15 Pct Recovery = 91% Analysis Date = 05/30/15 Pct Recovery = 91% Analysis Date = 05/25/15 Pct Recovery = 91% Analysis Date = 05/25/15 Pct Recovery = 91% Analysis Date = 05/21/15 Pct Recovery = 91% Analysis Date = 05/21/15 Pct Recovery = 91% Analysis Date = 05/16/15 Pct Recovery = 91% Analysis Date = 05/16/15 Pct Recovery = 91% Analysis Date = 05/11/15 Pct Recovery = 91% Analysis Date = 05/11/15 Pct Recovery = 91% Analysis Date = 05/06/15 Pct Recovery = 91% Analysis Date = 05/06/15 Pct Recovery = 91% Analysis Date = 05/02/15 Pct Recovery = 91% Analysis Date = 05/02/15 Pct Recovery = 91% Analysis Date = 04/27/15 Pct Recovery = 90% Analysis Date = 04/27/15 Pct Recovery = 90% Analysis Date = 04/22/15 Pct Recovery = 90% Analysis Date = 04/22/15 Pct Recovery = 90% Analysis Date = 04/17/15 Pct Recovery = 90% Analysis Date = 04/17/15 Pct Recovery = 90% Analysis Date = 04/12/15 Pct Recovery = 90% Analysis Date = 04/12/15 Pct Recovery = 90% Analysis Date = 04/08/15 Pct Recovery = 90% Analysis Date = 04/08/15 Pct Recovery = 90% Analysis Date = 04/03/15 Pct Recovery = 90% Analysis Date = 04/03/15 Pct Recovery = 90% Analysis Date = 03/29/15 Pct Recovery = 90% Analysis Date = 03/29/15 Pct Recovery = 90% Analysis Date = 03/24/15 Pct Recovery = 90% Analysis Date = 03/24/15 Pct Recovery = 90% Analysis Date = 03/19/15 Pct Recovery = 90% Analysis Date = 03/19/15 Pct Recovery = 90% Analysis Date = 03/15/15 Pct Recovery = 90% Analysis Date = 03/15/15 Pct Recovery = 90% Analysis Date = 03/10/15 Pct Recovery = 90% Analysis Date = 03/10/15 Pct Recovery = 90% Analysis Date = 03/05/15 Pct Recovery = 90% Analysis Date = 03/05/15 Pct Recovery = 90% Analysis Date = 02/28/15 Pct Recovery = 90% Analysis Date = 02/28/15 Pct Recovery = 90% Analysis Date = 02/23/15 Pct Recovery = 90% Analysis Date = 02/23/15 Pct Recovery = 90% Analysis Date = 02/19/15 Pct Recovery = 90% Analysis Date = 02/19/15 Pct Recovery = 90% Analysis Date = 02/14/15 Pct Recovery = 90% Analysis Date = 02/14/15 Pct Recovery = 90% Analysis Date = 02/09/15 Pct Recovery = 90% Analysis Date = 02/09/15 Pct Recovery = 90% Analysis Date = 02/04/15 Pct Recovery = 90% Analysis Date = 02/04/15 Pct Recovery = 90% Analysis Date = 01/31/15 Pct Recovery = 90% Analysis Date = 01/31/15 Pct Recovery = 90% Analysis Date = 01/26/15 Pct Recovery = 89% Analysis Date = 01/26/15 Pct Recovery = 89% Analysis Date = 01/21/15 Pct Recovery = 89% Analysis Date = 01/21/15 Pct Recovery = 89% Analysis Date = 01/16/15 Pct Recovery = 89% Analysis Date = 01/16/15 Pct Recovery = 89% Analysis Date = 01/11/15 Pct Recovery = 89% Analysis Date = 01/11/15 Pct Recovery = 89% Analysis Date = 01/07/15 Pct Recovery = 89% Analysis Date = 01/07/15 Pct Recovery = 89% Analysis Date = 01/02/15 Pct Recovery = 89% Analysis Date = 01/02/15 Pct Recovery = 89% Analysis Date = 12/28/14 Pct Recovery = 89% Analysis Date = 12/28/14 Pct Recovery = 89% Analysis Date = 12/23/14 Pct Recovery = 89% Analysis Date = 12/23/14 Pct Recovery = 89% Analysis Date = 12/18/14 Pct Recovery = 89% Analysis Date = 12/18/14 Pct Recovery = 89% Analysis Date = 12/14/14 Pct Recovery = 89% Analysis Date = 12/14/14 Pct Recovery = 89% Analysis Date = 12/09/14 Pct Recovery = 89% Analysis Date = 12/09/14 Pct Recovery = 89% Analysis Date = 12/04/14 Pct Recovery = 89% Analysis Date = 12/04/14 Pct Recovery = 89% Analysis Date = 11/29/14 Pct Recovery = 89% Analysis Date = 11/29/14 Pct Recovery = 89% Analysis Date = 11/24/14 Pct Recovery = 89% Analysis Date = 11/24/14 Pct Recovery = 89% Analysis Date = 11/20/14 Pct Recovery = 89% Analysis Date = 11/20/14 Pct Recovery = 89% Analysis Date = 11/15/14 Pct Recovery = 89% Analysis Date = 11/15/14 Pct Recovery = 89% Analysis Date = 11/10/14 Pct Recovery = 89% Analysis Date = 11/10/14 Pct Recovery = 89% Analysis Date = 11/05/14 Pct Recovery = 88% Analysis Date = 11/05/14 Pct Recovery = 88% Analysis Date = 11/01/14 Pct Recovery = 88% Analysis Date = 11/01/14 Pct Recovery = 88% Analysis Date = 10/27/14 Pct Recovery = 88% Analysis Date = 10/27/14 Pct Recovery = 88% Analysis Date = 10/22/14 Pct Recovery = 88% Analysis Date = 10/22/14 Pct Recovery = 88% Analysis Date = 10/17/14 Pct Recovery = 88% Analysis Date = 10/17/14 Pct Recovery = 88% Analysis Date = 10/12/14 Pct Recovery = 88% Analysis Date = 10/12/14 Pct Recovery = 88% Analysis Date = 10/08/14 Pct Recovery = 88% Analysis Date = 10/08/14 Pct Recovery = 88% Analysis Date = 10/03/14 Pct Recovery = 88% Analysis Date = 10/03/14 Pct Recovery = 88% Analysis Date = 09/28/14 Pct Recovery = 88% Analysis Date = 09/28/14 Pct Recovery = 88% Analysis Date = 09/23/14 Pct Recovery = 88% Analysis Date = 09/23/14 Pct Recovery = 88% Analysis Date = 09/18/14 Pct Recovery = 88% Analysis Date = 09/18/14 Pct Recovery = 88% Analysis Date = 09/14/14 Pct Recovery = 88% Analysis Date = 09/14/14 Pct Recovery = 88% Analysis Date = 09/09/14 Pct Recovery = 88% Analysis Date = 09/09/14 Pct Recovery = 88% Analysis Date = 09/04/14 Pct Recovery = 87% Analysis Date = 09/04/14 Pct Recovery = 87% Analysis Date = 08/30/14 Pct Recovery = 87% Analysis Date = 08/30/14 Pct Recovery = 87% Analysis Date = 08/25/14 Pct Recovery = 87% Analysis Date = 08/25/14 Pct Recovery = 87% Analysis Date = 08/21/14 Pct Recovery = 87% Analysis Date = 08/21/14 Pct Recovery = 87% Analysis Date = 08/16/14 Pct Recovery = 87% Analysis Date = 08/16/14 Pct Recovery = 87% Analysis Date = 08/11/14 Pct Recovery = 87% Analysis Date = 08/11/14 Pct Recovery = 87% Analysis Date = 08/06/14 Pct Recovery = 87% Analysis Date = 08/06/14 Pct Recovery = 87% Analysis Date = 08/02/14 Pct Recovery = 87% Analysis Date = 08/02/14 Pct Recovery = 87% Analysis Date = 07/28/14 Pct Recovery = 87% Analysis Date = 07/28/14 Pct Recovery = 87% Analysis Date = 07/23/14 Pct Recovery = 87% Analysis Date = 07/23/14 Pct Recovery = 87% Analysis Date = 07/18/14 Pct Recovery = 87% Analysis Date = 07/18/14 Pct Recovery = 87% Analysis Date = 07/13/14 Pct Recovery = 87% Analysis Date = 07/13/14 Pct Recovery = 87% Analysis Date = 07/09/14 Pct Recovery = 87% Analysis Date = 07/09/14 Pct Recovery = 87% Analysis Date = 07/04/14 Pct Recovery = 86% Analysis Date = 07/04/14 Pct Recovery = 86% Analysis Date = 06/29/14 Pct Recovery = 86% Analysis Date = 06/29/14 Pct Recovery = 86% Analysis Date = 06/24/14 Pct Recovery = 86% Analysis Date = 06/24/14 Pct Recovery = 86% Analysis Date = 06/19/14 Pct Recovery = 86% Analysis Date = 06/19/14 Pct Recovery = 86% Analysis Date = 06/15/14 Pct Recovery = 86% Analysis Date = 06/15/14 Pct Recovery = 86% Analysis Date = 06/10/14 Pct Recovery = 86% Analysis Date = 06/10/14 Pct Recovery = 86% Analysis Date = 06/05/14 Pct Recovery = 86% Analysis Date = 06/05/14 Pct Recovery = 86% Analysis Date = 05/31/14 Pct Recovery = 86% Analysis Date = 05/31/14 Pct Recovery = 86% Analysis Date = 05/26/14 Pct Recovery = 86% Analysis Date = 05/26/14 Pct Recovery = 86% Analysis Date = 05/22/14 Pct Recovery = 86% Analysis Date = 05/22/14 Pct Recovery = 86% Analysis Date = 05/17/14 Pct Recovery = 86% Analysis Date = 05/17/14 Pct Recovery = 86% Analysis Date = 05/12/14 Pct Recovery = 86% Analysis Date = 05/12/14 Pct Recovery = 86% Analysis Date = 05/07/14 Pct Recovery = 86% Analysis Date = 05/07/14 Pct Recovery = 86% Analysis Date = 05/03/14 Pct Recovery = 85% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
SEC-BUTYLBENZENE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 50 90% 11% 90% 11%
Total 50 90% 11% 90% 11%

Sample Statistics
SEC-BUTYLBENZENE

Characteristic N % % Basis
Plotted 50 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 50 .  
False Negatives 0 0% 0 out of 50
Not Spiked 23 .  
False Positives 0 0% 0 out of 23

BQS OBSP Determination:
STYRENE
METHOD: 4440 , TESTIDCODE: 77128GCM66
Open Data Set

Analysis Date = 12/16/16 SpikeMix = NSI 041816AVOC: 40 µl & ChemService 5082900: 40 µl Pct Recovery = 100% Analysis Date = 12/12/16 SpikeMix = Accu 216041125: 40 µl & Crescent 03FF058: 40 µl Pct Recovery = 96% Analysis Date = 08/04/16 SpikeMix = Crescent 03FF058: 40 µl & Supelco LC20141V: 40 µl Pct Recovery = 89% Analysis Date = 07/14/16 SpikeMix = Accu 216041125: 40 µl & NSI 041816AVOC: 40 µl Pct Recovery = 90% Analysis Date = 11/21/16 SpikeMix = Crescent 03FF058: 25 µl & Supelco LC20141V: 25 µl Pct Recovery = 97% Analysis Date = 08/26/16 SpikeMix = NSI 041816AVOC: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 94% Analysis Date = 06/30/16 SpikeMix = Crescent 03FF058: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 87% Analysis Date = 06/21/16 SpikeMix = Phenova B20160319: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 92% Analysis Date = 05/24/16 SpikeMix = Accu 216041125: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 82% Analysis Date = 03/06/15 SpikeMix = ERA 0227-14-06.1A: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 91% Analysis Date = 12/17/14 SpikeMix = Supelco LC06438: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 98% Analysis Date = 09/21/14 SpikeMix = Supelco LC06438: 20 µl Pct Recovery = 90% Analysis Date = 06/10/14 SpikeMix = NSI 032614: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 89% Analysis Date = 03/19/15 SpikeMix = Spex Organics C1140417015: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 99% Analysis Date = 11/22/14 SpikeMix = NSI 032614: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 92% Analysis Date = 08/19/14 SpikeMix = Spex Organics C1140417015: 20 µl & Accu 214031115: 20 µl Pct Recovery = 98% Analysis Date = 08/16/14 SpikeMix = ERA 0227-14-06.1A: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 87% Analysis Date = 09/29/15 SpikeMix = Accu 215041380: 25 µl & ERA 0406-15-03: 25 µl Pct Recovery = 81% Analysis Date = 06/16/15 SpikeMix = ERA 0406-15-03: 25 µl & Supelco LC13545: 25 µl Pct Recovery = 78% Analysis Date = 07/13/15 SpikeMix = Crescent 04EE008: 25 µl & NSI 050515AVOC: 25 µl Pct Recovery = 84% Analysis Date = 10/13/16 SpikeMix = Accu 216041125: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 97% Analysis Date = 10/13/16 SpikeMix = NSI 041816AVOC: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 91% Analysis Date = 09/28/16 SpikeMix = Crescent 03FF058: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 88% Analysis Date = 09/08/16 SpikeMix = Phenova B20160319: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 78% Analysis Date = 08/20/16 SpikeMix = Accu 216041125: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 91% Analysis Date = 07/29/16 SpikeMix = Phenova B20160319: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 91% Analysis Date = 06/10/16 SpikeMix = NSI 041816AVOC: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 99% Analysis Date = 04/26/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 81% Analysis Date = 03/04/16 SpikeMix = Accu 215041380: 15 µl & ERA 0406-15-03: 15 µl Pct Recovery = 78% Analysis Date = 02/05/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 86% Analysis Date = 10/16/15 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 83% Analysis Date = 11/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 79% Analysis Date = 10/17/15 SpikeMix = Crescent 04EE008: 15 µl & NSI 050515AVOC: 15 µl Pct Recovery = 83% Analysis Date = 06/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Accu 215041380: 15 µl Pct Recovery = 88% Analysis Date = 10/21/14 SpikeMix = ERA 0227-14-06.1A: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 100% Analysis Date = 06/18/14 SpikeMix = Supelco LC06438: 10 µl & Accu 214031115: 10 µl Pct Recovery = 82% Analysis Date = 05/30/14 SpikeMix = NSI 032614: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 76% Analysis Date = 05/03/14 SpikeMix = Crescent 03DD004: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 112% Analysis Date = 11/06/14 SpikeMix = Spex Organics C1140417015: 10 µl & Crescent 03DD004: 10 µl Pct Recovery = 109% Analysis Date = 09/09/14 SpikeMix = NSI 032614: 10 µl & Spex Organics C1140417015: 10 µl Pct Recovery = 124% Analysis Date = 07/23/14 SpikeMix = Spex Organics C1140417015: 10 µl & Accu 214031115: 10 µl Pct Recovery = 110% Analysis Date = 07/11/14 SpikeMix = Spex Organics C1140417015: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 108% Analysis Date = 11/20/15 SpikeMix = Accu 215041380: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 84% Analysis Date = 07/31/15 SpikeMix = Crescent 04EE008: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 78% Analysis Date = 06/27/15 SpikeMix = ERA 0406-15-03: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 98% Analysis Date = 03/17/16 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 148% Analysis Date = 01/27/16 SpikeMix = Crescent 04EE008: 10 µl & NSI 050515AVOC: 10 µl Pct Recovery = 94% Analysis Date = 12/10/15 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 102% Analysis Date = 09/03/15 SpikeMix = NSI 050515AVOC: 10 µl & Spex Organics EN150428007: 10 µl Pct Recovery = 85% Analysis Date = 12/16/16 Pct Recovery = 93% Analysis Date = 12/11/16 Pct Recovery = 93% Analysis Date = 12/11/16 Pct Recovery = 93% Analysis Date = 12/06/16 Pct Recovery = 93% Analysis Date = 12/06/16 Pct Recovery = 93% Analysis Date = 12/01/16 Pct Recovery = 93% Analysis Date = 12/01/16 Pct Recovery = 93% Analysis Date = 11/26/16 Pct Recovery = 92% Analysis Date = 11/26/16 Pct Recovery = 92% Analysis Date = 11/22/16 Pct Recovery = 92% Analysis Date = 11/22/16 Pct Recovery = 92% Analysis Date = 11/17/16 Pct Recovery = 92% Analysis Date = 11/17/16 Pct Recovery = 92% Analysis Date = 11/12/16 Pct Recovery = 92% Analysis Date = 11/12/16 Pct Recovery = 92% Analysis Date = 11/07/16 Pct Recovery = 92% Analysis Date = 11/07/16 Pct Recovery = 92% Analysis Date = 11/02/16 Pct Recovery = 92% Analysis Date = 11/02/16 Pct Recovery = 92% Analysis Date = 10/29/16 Pct Recovery = 92% Analysis Date = 10/29/16 Pct Recovery = 92% Analysis Date = 10/24/16 Pct Recovery = 92% Analysis Date = 10/24/16 Pct Recovery = 92% Analysis Date = 10/19/16 Pct Recovery = 92% Analysis Date = 10/19/16 Pct Recovery = 92% Analysis Date = 10/14/16 Pct Recovery = 92% Analysis Date = 10/14/16 Pct Recovery = 92% Analysis Date = 10/09/16 Pct Recovery = 92% Analysis Date = 10/09/16 Pct Recovery = 92% Analysis Date = 10/05/16 Pct Recovery = 92% Analysis Date = 10/05/16 Pct Recovery = 92% Analysis Date = 09/30/16 Pct Recovery = 92% Analysis Date = 09/30/16 Pct Recovery = 92% Analysis Date = 09/25/16 Pct Recovery = 92% Analysis Date = 09/25/16 Pct Recovery = 92% Analysis Date = 09/20/16 Pct Recovery = 92% Analysis Date = 09/20/16 Pct Recovery = 92% Analysis Date = 09/15/16 Pct Recovery = 92% Analysis Date = 09/15/16 Pct Recovery = 92% Analysis Date = 09/11/16 Pct Recovery = 92% Analysis Date = 09/11/16 Pct Recovery = 92% Analysis Date = 09/06/16 Pct Recovery = 92% Analysis Date = 09/06/16 Pct Recovery = 92% Analysis Date = 09/01/16 Pct Recovery = 92% Analysis Date = 09/01/16 Pct Recovery = 92% Analysis Date = 08/27/16 Pct Recovery = 92% Analysis Date = 08/27/16 Pct Recovery = 92% Analysis Date = 08/23/16 Pct Recovery = 92% Analysis Date = 08/23/16 Pct Recovery = 92% Analysis Date = 08/18/16 Pct Recovery = 92% Analysis Date = 08/18/16 Pct Recovery = 92% Analysis Date = 08/13/16 Pct Recovery = 92% Analysis Date = 08/13/16 Pct Recovery = 92% Analysis Date = 08/08/16 Pct Recovery = 92% Analysis Date = 08/08/16 Pct Recovery = 92% Analysis Date = 08/03/16 Pct Recovery = 92% Analysis Date = 08/03/16 Pct Recovery = 92% Analysis Date = 07/30/16 Pct Recovery = 92% Analysis Date = 07/30/16 Pct Recovery = 92% Analysis Date = 07/25/16 Pct Recovery = 92% Analysis Date = 07/25/16 Pct Recovery = 92% Analysis Date = 07/20/16 Pct Recovery = 92% Analysis Date = 07/20/16 Pct Recovery = 92% Analysis Date = 07/15/16 Pct Recovery = 92% Analysis Date = 07/15/16 Pct Recovery = 92% Analysis Date = 07/10/16 Pct Recovery = 92% Analysis Date = 07/10/16 Pct Recovery = 92% Analysis Date = 07/06/16 Pct Recovery = 92% Analysis Date = 07/06/16 Pct Recovery = 92% Analysis Date = 07/01/16 Pct Recovery = 92% Analysis Date = 07/01/16 Pct Recovery = 92% Analysis Date = 06/26/16 Pct Recovery = 92% Analysis Date = 06/26/16 Pct Recovery = 92% Analysis Date = 06/21/16 Pct Recovery = 92% Analysis Date = 06/21/16 Pct Recovery = 92% Analysis Date = 06/16/16 Pct Recovery = 92% Analysis Date = 06/16/16 Pct Recovery = 92% Analysis Date = 06/12/16 Pct Recovery = 92% Analysis Date = 06/12/16 Pct Recovery = 92% Analysis Date = 06/07/16 Pct Recovery = 92% Analysis Date = 06/07/16 Pct Recovery = 92% Analysis Date = 06/02/16 Pct Recovery = 92% Analysis Date = 06/02/16 Pct Recovery = 92% Analysis Date = 05/28/16 Pct Recovery = 92% Analysis Date = 05/28/16 Pct Recovery = 92% Analysis Date = 05/24/16 Pct Recovery = 92% Analysis Date = 05/24/16 Pct Recovery = 92% Analysis Date = 05/19/16 Pct Recovery = 92% Analysis Date = 05/19/16 Pct Recovery = 92% Analysis Date = 05/14/16 Pct Recovery = 92% Analysis Date = 05/14/16 Pct Recovery = 92% Analysis Date = 05/09/16 Pct Recovery = 92% Analysis Date = 05/09/16 Pct Recovery = 92% Analysis Date = 05/04/16 Pct Recovery = 92% Analysis Date = 05/04/16 Pct Recovery = 92% Analysis Date = 04/30/16 Pct Recovery = 92% Analysis Date = 04/30/16 Pct Recovery = 92% Analysis Date = 04/25/16 Pct Recovery = 92% Analysis Date = 04/25/16 Pct Recovery = 92% Analysis Date = 04/20/16 Pct Recovery = 91% Analysis Date = 04/20/16 Pct Recovery = 91% Analysis Date = 04/15/16 Pct Recovery = 91% Analysis Date = 04/15/16 Pct Recovery = 91% Analysis Date = 04/10/16 Pct Recovery = 91% Analysis Date = 04/10/16 Pct Recovery = 91% Analysis Date = 04/06/16 Pct Recovery = 91% Analysis Date = 04/06/16 Pct Recovery = 91% Analysis Date = 04/01/16 Pct Recovery = 91% Analysis Date = 04/01/16 Pct Recovery = 91% Analysis Date = 03/27/16 Pct Recovery = 91% Analysis Date = 03/27/16 Pct Recovery = 91% Analysis Date = 03/22/16 Pct Recovery = 91% Analysis Date = 03/22/16 Pct Recovery = 91% Analysis Date = 03/17/16 Pct Recovery = 91% Analysis Date = 03/17/16 Pct Recovery = 91% Analysis Date = 03/13/16 Pct Recovery = 91% Analysis Date = 03/13/16 Pct Recovery = 91% Analysis Date = 03/08/16 Pct Recovery = 91% Analysis Date = 03/08/16 Pct Recovery = 91% Analysis Date = 03/03/16 Pct Recovery = 91% Analysis Date = 03/03/16 Pct Recovery = 91% Analysis Date = 02/27/16 Pct Recovery = 91% Analysis Date = 02/27/16 Pct Recovery = 91% Analysis Date = 02/23/16 Pct Recovery = 91% Analysis Date = 02/23/16 Pct Recovery = 91% Analysis Date = 02/18/16 Pct Recovery = 91% Analysis Date = 02/18/16 Pct Recovery = 91% Analysis Date = 02/13/16 Pct Recovery = 90% Analysis Date = 02/13/16 Pct Recovery = 90% Analysis Date = 02/08/16 Pct Recovery = 90% Analysis Date = 02/08/16 Pct Recovery = 90% Analysis Date = 02/03/16 Pct Recovery = 90% Analysis Date = 02/03/16 Pct Recovery = 90% Analysis Date = 01/30/16 Pct Recovery = 90% Analysis Date = 01/30/16 Pct Recovery = 90% Analysis Date = 01/25/16 Pct Recovery = 90% Analysis Date = 01/25/16 Pct Recovery = 90% Analysis Date = 01/20/16 Pct Recovery = 90% Analysis Date = 01/20/16 Pct Recovery = 90% Analysis Date = 01/15/16 Pct Recovery = 90% Analysis Date = 01/15/16 Pct Recovery = 90% Analysis Date = 01/10/16 Pct Recovery = 90% Analysis Date = 01/10/16 Pct Recovery = 90% Analysis Date = 01/06/16 Pct Recovery = 90% Analysis Date = 01/06/16 Pct Recovery = 90% Analysis Date = 01/01/16 Pct Recovery = 90% Analysis Date = 01/01/16 Pct Recovery = 90% Analysis Date = 12/27/15 Pct Recovery = 90% Analysis Date = 12/27/15 Pct Recovery = 90% Analysis Date = 12/22/15 Pct Recovery = 89% Analysis Date = 12/22/15 Pct Recovery = 89% Analysis Date = 12/17/15 Pct Recovery = 89% Analysis Date = 12/17/15 Pct Recovery = 89% Analysis Date = 12/13/15 Pct Recovery = 89% Analysis Date = 12/13/15 Pct Recovery = 89% Analysis Date = 12/08/15 Pct Recovery = 89% Analysis Date = 12/08/15 Pct Recovery = 89% Analysis Date = 12/03/15 Pct Recovery = 89% Analysis Date = 12/03/15 Pct Recovery = 89% Analysis Date = 11/28/15 Pct Recovery = 89% Analysis Date = 11/28/15 Pct Recovery = 89% Analysis Date = 11/24/15 Pct Recovery = 89% Analysis Date = 11/24/15 Pct Recovery = 89% Analysis Date = 11/19/15 Pct Recovery = 89% Analysis Date = 11/19/15 Pct Recovery = 89% Analysis Date = 11/14/15 Pct Recovery = 89% Analysis Date = 11/14/15 Pct Recovery = 89% Analysis Date = 11/09/15 Pct Recovery = 89% Analysis Date = 11/09/15 Pct Recovery = 89% Analysis Date = 11/04/15 Pct Recovery = 89% Analysis Date = 11/04/15 Pct Recovery = 89% Analysis Date = 10/31/15 Pct Recovery = 88% Analysis Date = 10/31/15 Pct Recovery = 88% Analysis Date = 10/26/15 Pct Recovery = 88% Analysis Date = 10/26/15 Pct Recovery = 88% Analysis Date = 10/21/15 Pct Recovery = 88% Analysis Date = 10/21/15 Pct Recovery = 88% Analysis Date = 10/16/15 Pct Recovery = 88% Analysis Date = 10/16/15 Pct Recovery = 88% Analysis Date = 10/11/15 Pct Recovery = 88% Analysis Date = 10/11/15 Pct Recovery = 88% Analysis Date = 10/07/15 Pct Recovery = 88% Analysis Date = 10/07/15 Pct Recovery = 88% Analysis Date = 10/02/15 Pct Recovery = 88% Analysis Date = 10/02/15 Pct Recovery = 88% Analysis Date = 09/27/15 Pct Recovery = 88% Analysis Date = 09/27/15 Pct Recovery = 88% Analysis Date = 09/22/15 Pct Recovery = 88% Analysis Date = 09/22/15 Pct Recovery = 88% Analysis Date = 09/17/15 Pct Recovery = 88% Analysis Date = 09/17/15 Pct Recovery = 88% Analysis Date = 09/13/15 Pct Recovery = 88% Analysis Date = 09/13/15 Pct Recovery = 88% Analysis Date = 09/08/15 Pct Recovery = 88% Analysis Date = 09/08/15 Pct Recovery = 88% Analysis Date = 09/03/15 Pct Recovery = 88% Analysis Date = 09/03/15 Pct Recovery = 88% Analysis Date = 08/29/15 Pct Recovery = 88% Analysis Date = 08/29/15 Pct Recovery = 88% Analysis Date = 08/25/15 Pct Recovery = 88% Analysis Date = 08/25/15 Pct Recovery = 88% Analysis Date = 08/20/15 Pct Recovery = 88% Analysis Date = 08/20/15 Pct Recovery = 88% Analysis Date = 08/15/15 Pct Recovery = 88% Analysis Date = 08/15/15 Pct Recovery = 88% Analysis Date = 08/10/15 Pct Recovery = 88% Analysis Date = 08/10/15 Pct Recovery = 88% Analysis Date = 08/05/15 Pct Recovery = 88% Analysis Date = 08/05/15 Pct Recovery = 88% Analysis Date = 08/01/15 Pct Recovery = 88% Analysis Date = 08/01/15 Pct Recovery = 88% Analysis Date = 07/27/15 Pct Recovery = 88% Analysis Date = 07/27/15 Pct Recovery = 88% Analysis Date = 07/22/15 Pct Recovery = 89% Analysis Date = 07/22/15 Pct Recovery = 89% Analysis Date = 07/17/15 Pct Recovery = 89% Analysis Date = 07/17/15 Pct Recovery = 89% Analysis Date = 07/12/15 Pct Recovery = 89% Analysis Date = 07/12/15 Pct Recovery = 89% Analysis Date = 07/08/15 Pct Recovery = 89% Analysis Date = 07/08/15 Pct Recovery = 89% Analysis Date = 07/03/15 Pct Recovery = 89% Analysis Date = 07/03/15 Pct Recovery = 89% Analysis Date = 06/28/15 Pct Recovery = 89% Analysis Date = 06/28/15 Pct Recovery = 89% Analysis Date = 06/23/15 Pct Recovery = 89% Analysis Date = 06/23/15 Pct Recovery = 89% Analysis Date = 06/18/15 Pct Recovery = 89% Analysis Date = 06/18/15 Pct Recovery = 89% Analysis Date = 06/14/15 Pct Recovery = 89% Analysis Date = 06/14/15 Pct Recovery = 89% Analysis Date = 06/09/15 Pct Recovery = 90% Analysis Date = 06/09/15 Pct Recovery = 90% Analysis Date = 06/04/15 Pct Recovery = 90% Analysis Date = 06/04/15 Pct Recovery = 90% Analysis Date = 05/30/15 Pct Recovery = 90% Analysis Date = 05/30/15 Pct Recovery = 90% Analysis Date = 05/25/15 Pct Recovery = 90% Analysis Date = 05/25/15 Pct Recovery = 90% Analysis Date = 05/21/15 Pct Recovery = 90% Analysis Date = 05/21/15 Pct Recovery = 90% Analysis Date = 05/16/15 Pct Recovery = 90% Analysis Date = 05/16/15 Pct Recovery = 90% Analysis Date = 05/11/15 Pct Recovery = 91% Analysis Date = 05/11/15 Pct Recovery = 91% Analysis Date = 05/06/15 Pct Recovery = 91% Analysis Date = 05/06/15 Pct Recovery = 91% Analysis Date = 05/02/15 Pct Recovery = 91% Analysis Date = 05/02/15 Pct Recovery = 91% Analysis Date = 04/27/15 Pct Recovery = 91% Analysis Date = 04/27/15 Pct Recovery = 91% Analysis Date = 04/22/15 Pct Recovery = 91% Analysis Date = 04/22/15 Pct Recovery = 91% Analysis Date = 04/17/15 Pct Recovery = 91% Analysis Date = 04/17/15 Pct Recovery = 91% Analysis Date = 04/12/15 Pct Recovery = 91% Analysis Date = 04/12/15 Pct Recovery = 91% Analysis Date = 04/08/15 Pct Recovery = 92% Analysis Date = 04/08/15 Pct Recovery = 92% Analysis Date = 04/03/15 Pct Recovery = 92% Analysis Date = 04/03/15 Pct Recovery = 92% Analysis Date = 03/29/15 Pct Recovery = 92% Analysis Date = 03/29/15 Pct Recovery = 92% Analysis Date = 03/24/15 Pct Recovery = 92% Analysis Date = 03/24/15 Pct Recovery = 92% Analysis Date = 03/19/15 Pct Recovery = 92% Analysis Date = 03/19/15 Pct Recovery = 92% Analysis Date = 03/15/15 Pct Recovery = 92% Analysis Date = 03/15/15 Pct Recovery = 92% Analysis Date = 03/10/15 Pct Recovery = 93% Analysis Date = 03/10/15 Pct Recovery = 93% Analysis Date = 03/05/15 Pct Recovery = 93% Analysis Date = 03/05/15 Pct Recovery = 93% Analysis Date = 02/28/15 Pct Recovery = 93% Analysis Date = 02/28/15 Pct Recovery = 93% Analysis Date = 02/23/15 Pct Recovery = 93% Analysis Date = 02/23/15 Pct Recovery = 93% Analysis Date = 02/19/15 Pct Recovery = 93% Analysis Date = 02/19/15 Pct Recovery = 93% Analysis Date = 02/14/15 Pct Recovery = 93% Analysis Date = 02/14/15 Pct Recovery = 93% Analysis Date = 02/09/15 Pct Recovery = 93% Analysis Date = 02/09/15 Pct Recovery = 93% Analysis Date = 02/04/15 Pct Recovery = 93% Analysis Date = 02/04/15 Pct Recovery = 93% Analysis Date = 01/31/15 Pct Recovery = 93% Analysis Date = 01/31/15 Pct Recovery = 93% Analysis Date = 01/26/15 Pct Recovery = 94% Analysis Date = 01/26/15 Pct Recovery = 94% Analysis Date = 01/21/15 Pct Recovery = 94% Analysis Date = 01/21/15 Pct Recovery = 94% Analysis Date = 01/16/15 Pct Recovery = 94% Analysis Date = 01/16/15 Pct Recovery = 94% Analysis Date = 01/11/15 Pct Recovery = 94% Analysis Date = 01/11/15 Pct Recovery = 94% Analysis Date = 01/07/15 Pct Recovery = 94% Analysis Date = 01/07/15 Pct Recovery = 94% Analysis Date = 01/02/15 Pct Recovery = 94% Analysis Date = 01/02/15 Pct Recovery = 94% Analysis Date = 12/28/14 Pct Recovery = 94% Analysis Date = 12/28/14 Pct Recovery = 94% Analysis Date = 12/23/14 Pct Recovery = 94% Analysis Date = 12/23/14 Pct Recovery = 94% Analysis Date = 12/18/14 Pct Recovery = 95% Analysis Date = 12/18/14 Pct Recovery = 95% Analysis Date = 12/14/14 Pct Recovery = 95% Analysis Date = 12/14/14 Pct Recovery = 95% Analysis Date = 12/09/14 Pct Recovery = 95% Analysis Date = 12/09/14 Pct Recovery = 95% Analysis Date = 12/04/14 Pct Recovery = 95% Analysis Date = 12/04/14 Pct Recovery = 95% Analysis Date = 11/29/14 Pct Recovery = 95% Analysis Date = 11/29/14 Pct Recovery = 95% Analysis Date = 11/24/14 Pct Recovery = 95% Analysis Date = 11/24/14 Pct Recovery = 95% Analysis Date = 11/20/14 Pct Recovery = 95% Analysis Date = 11/20/14 Pct Recovery = 95% Analysis Date = 11/15/14 Pct Recovery = 95% Analysis Date = 11/15/14 Pct Recovery = 95% Analysis Date = 11/10/14 Pct Recovery = 95% Analysis Date = 11/10/14 Pct Recovery = 95% Analysis Date = 11/05/14 Pct Recovery = 96% Analysis Date = 11/05/14 Pct Recovery = 96% Analysis Date = 11/01/14 Pct Recovery = 96% Analysis Date = 11/01/14 Pct Recovery = 96% Analysis Date = 10/27/14 Pct Recovery = 96% Analysis Date = 10/27/14 Pct Recovery = 96% Analysis Date = 10/22/14 Pct Recovery = 96% Analysis Date = 10/22/14 Pct Recovery = 96% Analysis Date = 10/17/14 Pct Recovery = 96% Analysis Date = 10/17/14 Pct Recovery = 96% Analysis Date = 10/12/14 Pct Recovery = 96% Analysis Date = 10/12/14 Pct Recovery = 96% Analysis Date = 10/08/14 Pct Recovery = 96% Analysis Date = 10/08/14 Pct Recovery = 96% Analysis Date = 10/03/14 Pct Recovery = 96% Analysis Date = 10/03/14 Pct Recovery = 96% Analysis Date = 09/28/14 Pct Recovery = 97% Analysis Date = 09/28/14 Pct Recovery = 97% Analysis Date = 09/23/14 Pct Recovery = 97% Analysis Date = 09/23/14 Pct Recovery = 97% Analysis Date = 09/18/14 Pct Recovery = 97% Analysis Date = 09/18/14 Pct Recovery = 97% Analysis Date = 09/14/14 Pct Recovery = 97% Analysis Date = 09/14/14 Pct Recovery = 97% Analysis Date = 09/09/14 Pct Recovery = 97% Analysis Date = 09/09/14 Pct Recovery = 97% Analysis Date = 09/04/14 Pct Recovery = 97% Analysis Date = 09/04/14 Pct Recovery = 97% Analysis Date = 08/30/14 Pct Recovery = 97% Analysis Date = 08/30/14 Pct Recovery = 97% Analysis Date = 08/25/14 Pct Recovery = 97% Analysis Date = 08/25/14 Pct Recovery = 97% Analysis Date = 08/21/14 Pct Recovery = 98% Analysis Date = 08/21/14 Pct Recovery = 98% Analysis Date = 08/16/14 Pct Recovery = 98% Analysis Date = 08/16/14 Pct Recovery = 98% Analysis Date = 08/11/14 Pct Recovery = 98% Analysis Date = 08/11/14 Pct Recovery = 98% Analysis Date = 08/06/14 Pct Recovery = 98% Analysis Date = 08/06/14 Pct Recovery = 98% Analysis Date = 08/02/14 Pct Recovery = 98% Analysis Date = 08/02/14 Pct Recovery = 98% Analysis Date = 07/28/14 Pct Recovery = 98% Analysis Date = 07/28/14 Pct Recovery = 98% Analysis Date = 07/23/14 Pct Recovery = 98% Analysis Date = 07/23/14 Pct Recovery = 98% Analysis Date = 07/18/14 Pct Recovery = 98% Analysis Date = 07/18/14 Pct Recovery = 98% Analysis Date = 07/13/14 Pct Recovery = 98% Analysis Date = 07/13/14 Pct Recovery = 98% Analysis Date = 07/09/14 Pct Recovery = 98% Analysis Date = 07/09/14 Pct Recovery = 98% Analysis Date = 07/04/14 Pct Recovery = 99% Analysis Date = 07/04/14 Pct Recovery = 99% Analysis Date = 06/29/14 Pct Recovery = 99% Analysis Date = 06/29/14 Pct Recovery = 99% Analysis Date = 06/24/14 Pct Recovery = 99% Analysis Date = 06/24/14 Pct Recovery = 99% Analysis Date = 06/19/14 Pct Recovery = 99% Analysis Date = 06/19/14 Pct Recovery = 99% Analysis Date = 06/15/14 Pct Recovery = 99% Analysis Date = 06/15/14 Pct Recovery = 99% Analysis Date = 06/10/14 Pct Recovery = 99% Analysis Date = 06/10/14 Pct Recovery = 99% Analysis Date = 06/05/14 Pct Recovery = 99% Analysis Date = 06/05/14 Pct Recovery = 99% Analysis Date = 05/31/14 Pct Recovery = 99% Analysis Date = 05/31/14 Pct Recovery = 99% Analysis Date = 05/26/14 Pct Recovery = 99% Analysis Date = 05/26/14 Pct Recovery = 99% Analysis Date = 05/22/14 Pct Recovery = 99% Analysis Date = 05/22/14 Pct Recovery = 99% Analysis Date = 05/17/14 Pct Recovery = 100% Analysis Date = 05/17/14 Pct Recovery = 100% Analysis Date = 05/12/14 Pct Recovery = 100% Analysis Date = 05/12/14 Pct Recovery = 100% Analysis Date = 05/07/14 Pct Recovery = 100% Analysis Date = 05/07/14 Pct Recovery = 100% Analysis Date = 05/03/14 Pct Recovery = 100% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
STYRENE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 49 93% 13% 91% 10%
Total 49 93% 13% 91% 10%

Sample Statistics
STYRENE

Characteristic N % % Basis
Plotted 49 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 49 .  
False Negatives 0 0% 0 out of 49
Not Spiked 24 .  
False Positives 0 0% 0 out of 24

BQS OBSP Determination:
TERT-BUTYLBENZENE
METHOD: 4440 , TESTIDCODE: 77353GCM66
Open Data Set

Analysis Date = 12/12/16 SpikeMix = Accu 216041125: 40 µl & Crescent 03FF058: 40 µl Pct Recovery = 104% Analysis Date = 07/20/16 SpikeMix = Supelco LC20141V: 40 µl & Accu 216041125: 40 µl Pct Recovery = 92% Analysis Date = 07/14/16 SpikeMix = Accu 216041125: 40 µl & NSI 041816AVOC: 40 µl Pct Recovery = 83% Analysis Date = 08/12/16 SpikeMix = ChemService 5082900: 25 µl & Phenova B20160319: 25 µl Pct Recovery = 80% Analysis Date = 06/21/16 SpikeMix = Phenova B20160319: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 101% Analysis Date = 09/08/16 SpikeMix = Supelco LC20141V: 25 µl & Accu 216041125: 25 µl Pct Recovery = 72% Analysis Date = 05/24/16 SpikeMix = Accu 216041125: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 87% Analysis Date = 03/19/15 SpikeMix = Spex Organics C1140417015: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 84% Analysis Date = 12/17/14 SpikeMix = Supelco LC06438: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 75% Analysis Date = 11/14/14 SpikeMix = Crescent 03DD004: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 72% Analysis Date = 06/10/14 SpikeMix = Crescent 03DD004: 20 µl & NSI 032614: 20 µl Pct Recovery = 74% Analysis Date = 04/09/15 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 79% Analysis Date = 08/19/14 SpikeMix = Spex Organics C1140417015: 20 µl & Accu 214031115: 20 µl Pct Recovery = 80% Analysis Date = 07/01/14 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 77% Analysis Date = 05/01/14 SpikeMix = Accu 214031115: 20 µl & NSI 032614: 20 µl Pct Recovery = 72% Analysis Date = 08/15/15 SpikeMix = Supelco LC13545: 25 µl & Crescent 04EE008: 25 µl Pct Recovery = 98% Analysis Date = 06/16/15 SpikeMix = ERA 0406-15-03: 25 µl & Supelco LC13545: 25 µl Pct Recovery = 84% Analysis Date = 11/29/16 SpikeMix = ChemService 5082900: 15 µl & Phenova B20160319: 15 µl Pct Recovery = 86% Analysis Date = 09/08/16 SpikeMix = Phenova B20160319: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 84% Analysis Date = 07/29/16 SpikeMix = Phenova B20160319: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 90% Analysis Date = 05/27/16 SpikeMix = Phenova B20160319: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 84% Analysis Date = 10/13/16 SpikeMix = Accu 216041125: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 88% Analysis Date = 08/20/16 SpikeMix = Accu 216041125: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 85% Analysis Date = 06/30/16 SpikeMix = ChemService 5082900: 15 µl & Accu 216041125: 15 µl Pct Recovery = 59% Analysis Date = 04/26/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 78% Analysis Date = 02/05/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 90% Analysis Date = 11/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 79% Analysis Date = 10/16/15 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 80% Analysis Date = 05/09/15 SpikeMix = Spex Organics EN150428007: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 90% Analysis Date = 04/02/16 SpikeMix = Supelco LC13545: 15 µl & Accu 215041380: 15 µl Pct Recovery = 88% Analysis Date = 12/18/15 SpikeMix = Supelco LC13545: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 78% Analysis Date = 11/06/14 SpikeMix = Spex Organics C1140417015: 10 µl & Crescent 03DD004: 10 µl Pct Recovery = 82% Analysis Date = 10/04/14 SpikeMix = Crescent 03DD004: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 77% Analysis Date = 07/29/14 SpikeMix = Crescent 03DD004: 10 µl & NSI 032614: 10 µl Pct Recovery = 83% Analysis Date = 05/03/14 SpikeMix = Crescent 03DD004: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 88% Analysis Date = 01/13/15 SpikeMix = Accu 214031115: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 79% Analysis Date = 09/09/14 SpikeMix = Accu 214031115: 10 µl & NSI 032614: 10 µl Pct Recovery = 92% Analysis Date = 07/23/14 SpikeMix = Spex Organics C1140417015: 10 µl & Accu 214031115: 10 µl Pct Recovery = 97% Analysis Date = 06/18/14 SpikeMix = Supelco LC06438: 10 µl & Accu 214031115: 10 µl Pct Recovery = 81% Analysis Date = 02/18/16 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 91% Analysis Date = 11/12/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 89% Analysis Date = 09/03/15 SpikeMix = NSI 050515AVOC: 10 µl & Spex Organics EN150428007: 10 µl Pct Recovery = 75% Analysis Date = 05/21/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 93% Analysis Date = 05/13/16 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 93% Analysis Date = 03/17/16 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 80% Analysis Date = 12/10/15 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 91% Analysis Date = 06/27/15 SpikeMix = ERA 0406-15-03: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 88% Analysis Date = 05/09/15 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 86% Analysis Date = 12/11/16 Pct Recovery = 88% Analysis Date = 12/07/16 Pct Recovery = 88% Analysis Date = 12/07/16 Pct Recovery = 88% Analysis Date = 12/02/16 Pct Recovery = 88% Analysis Date = 12/02/16 Pct Recovery = 88% Analysis Date = 11/27/16 Pct Recovery = 87% Analysis Date = 11/27/16 Pct Recovery = 87% Analysis Date = 11/22/16 Pct Recovery = 87% Analysis Date = 11/22/16 Pct Recovery = 87% Analysis Date = 11/18/16 Pct Recovery = 87% Analysis Date = 11/18/16 Pct Recovery = 87% Analysis Date = 11/13/16 Pct Recovery = 87% Analysis Date = 11/13/16 Pct Recovery = 87% Analysis Date = 11/08/16 Pct Recovery = 87% Analysis Date = 11/08/16 Pct Recovery = 87% Analysis Date = 11/03/16 Pct Recovery = 87% Analysis Date = 11/03/16 Pct Recovery = 87% Analysis Date = 10/29/16 Pct Recovery = 87% Analysis Date = 10/29/16 Pct Recovery = 87% Analysis Date = 10/25/16 Pct Recovery = 87% Analysis Date = 10/25/16 Pct Recovery = 87% Analysis Date = 10/20/16 Pct Recovery = 87% Analysis Date = 10/20/16 Pct Recovery = 87% Analysis Date = 10/15/16 Pct Recovery = 87% Analysis Date = 10/15/16 Pct Recovery = 87% Analysis Date = 10/10/16 Pct Recovery = 87% Analysis Date = 10/10/16 Pct Recovery = 87% Analysis Date = 10/06/16 Pct Recovery = 87% Analysis Date = 10/06/16 Pct Recovery = 87% Analysis Date = 10/01/16 Pct Recovery = 87% Analysis Date = 10/01/16 Pct Recovery = 87% Analysis Date = 09/26/16 Pct Recovery = 87% Analysis Date = 09/26/16 Pct Recovery = 87% Analysis Date = 09/21/16 Pct Recovery = 87% Analysis Date = 09/21/16 Pct Recovery = 87% Analysis Date = 09/16/16 Pct Recovery = 86% Analysis Date = 09/16/16 Pct Recovery = 86% Analysis Date = 09/12/16 Pct Recovery = 86% Analysis Date = 09/12/16 Pct Recovery = 86% Analysis Date = 09/07/16 Pct Recovery = 86% Analysis Date = 09/07/16 Pct Recovery = 86% Analysis Date = 09/02/16 Pct Recovery = 86% Analysis Date = 09/02/16 Pct Recovery = 86% Analysis Date = 08/28/16 Pct Recovery = 86% Analysis Date = 08/28/16 Pct Recovery = 86% Analysis Date = 08/24/16 Pct Recovery = 86% Analysis Date = 08/24/16 Pct Recovery = 86% Analysis Date = 08/19/16 Pct Recovery = 86% Analysis Date = 08/19/16 Pct Recovery = 86% Analysis Date = 08/14/16 Pct Recovery = 86% Analysis Date = 08/14/16 Pct Recovery = 86% Analysis Date = 08/09/16 Pct Recovery = 86% Analysis Date = 08/09/16 Pct Recovery = 86% Analysis Date = 08/04/16 Pct Recovery = 86% Analysis Date = 08/04/16 Pct Recovery = 86% Analysis Date = 07/31/16 Pct Recovery = 86% Analysis Date = 07/31/16 Pct Recovery = 86% Analysis Date = 07/26/16 Pct Recovery = 86% Analysis Date = 07/26/16 Pct Recovery = 86% Analysis Date = 07/21/16 Pct Recovery = 86% Analysis Date = 07/21/16 Pct Recovery = 86% Analysis Date = 07/16/16 Pct Recovery = 86% Analysis Date = 07/16/16 Pct Recovery = 86% Analysis Date = 07/12/16 Pct Recovery = 86% Analysis Date = 07/12/16 Pct Recovery = 86% Analysis Date = 07/07/16 Pct Recovery = 85% Analysis Date = 07/07/16 Pct Recovery = 85% Analysis Date = 07/02/16 Pct Recovery = 85% Analysis Date = 07/02/16 Pct Recovery = 85% Analysis Date = 06/27/16 Pct Recovery = 85% Analysis Date = 06/27/16 Pct Recovery = 85% Analysis Date = 06/22/16 Pct Recovery = 85% Analysis Date = 06/22/16 Pct Recovery = 85% Analysis Date = 06/18/16 Pct Recovery = 85% Analysis Date = 06/18/16 Pct Recovery = 85% Analysis Date = 06/13/16 Pct Recovery = 85% Analysis Date = 06/13/16 Pct Recovery = 85% Analysis Date = 06/08/16 Pct Recovery = 85% Analysis Date = 06/08/16 Pct Recovery = 85% Analysis Date = 06/03/16 Pct Recovery = 85% Analysis Date = 06/03/16 Pct Recovery = 85% Analysis Date = 05/30/16 Pct Recovery = 85% Analysis Date = 05/30/16 Pct Recovery = 85% Analysis Date = 05/25/16 Pct Recovery = 85% Analysis Date = 05/25/16 Pct Recovery = 85% Analysis Date = 05/20/16 Pct Recovery = 85% Analysis Date = 05/20/16 Pct Recovery = 85% Analysis Date = 05/15/16 Pct Recovery = 85% Analysis Date = 05/15/16 Pct Recovery = 85% Analysis Date = 05/10/16 Pct Recovery = 85% Analysis Date = 05/10/16 Pct Recovery = 85% Analysis Date = 05/06/16 Pct Recovery = 85% Analysis Date = 05/06/16 Pct Recovery = 85% Analysis Date = 05/01/16 Pct Recovery = 85% Analysis Date = 05/01/16 Pct Recovery = 85% Analysis Date = 04/26/16 Pct Recovery = 85% Analysis Date = 04/26/16 Pct Recovery = 85% Analysis Date = 04/21/16 Pct Recovery = 85% Analysis Date = 04/21/16 Pct Recovery = 85% Analysis Date = 04/16/16 Pct Recovery = 85% Analysis Date = 04/16/16 Pct Recovery = 85% Analysis Date = 04/12/16 Pct Recovery = 85% Analysis Date = 04/12/16 Pct Recovery = 85% Analysis Date = 04/07/16 Pct Recovery = 85% Analysis Date = 04/07/16 Pct Recovery = 85% Analysis Date = 04/02/16 Pct Recovery = 85% Analysis Date = 04/02/16 Pct Recovery = 85% Analysis Date = 03/28/16 Pct Recovery = 85% Analysis Date = 03/28/16 Pct Recovery = 85% Analysis Date = 03/24/16 Pct Recovery = 85% Analysis Date = 03/24/16 Pct Recovery = 85% Analysis Date = 03/19/16 Pct Recovery = 85% Analysis Date = 03/19/16 Pct Recovery = 85% Analysis Date = 03/14/16 Pct Recovery = 85% Analysis Date = 03/14/16 Pct Recovery = 85% Analysis Date = 03/09/16 Pct Recovery = 85% Analysis Date = 03/09/16 Pct Recovery = 85% Analysis Date = 03/04/16 Pct Recovery = 85% Analysis Date = 03/04/16 Pct Recovery = 85% Analysis Date = 02/29/16 Pct Recovery = 85% Analysis Date = 02/29/16 Pct Recovery = 85% Analysis Date = 02/24/16 Pct Recovery = 85% Analysis Date = 02/24/16 Pct Recovery = 85% Analysis Date = 02/19/16 Pct Recovery = 85% Analysis Date = 02/19/16 Pct Recovery = 85% Analysis Date = 02/14/16 Pct Recovery = 85% Analysis Date = 02/14/16 Pct Recovery = 85% Analysis Date = 02/10/16 Pct Recovery = 85% Analysis Date = 02/10/16 Pct Recovery = 85% Analysis Date = 02/05/16 Pct Recovery = 85% Analysis Date = 02/05/16 Pct Recovery = 85% Analysis Date = 01/31/16 Pct Recovery = 85% Analysis Date = 01/31/16 Pct Recovery = 85% Analysis Date = 01/26/16 Pct Recovery = 85% Analysis Date = 01/26/16 Pct Recovery = 85% Analysis Date = 01/21/16 Pct Recovery = 85% Analysis Date = 01/21/16 Pct Recovery = 85% Analysis Date = 01/17/16 Pct Recovery = 85% Analysis Date = 01/17/16 Pct Recovery = 85% Analysis Date = 01/12/16 Pct Recovery = 85% Analysis Date = 01/12/16 Pct Recovery = 85% Analysis Date = 01/07/16 Pct Recovery = 85% Analysis Date = 01/07/16 Pct Recovery = 85% Analysis Date = 01/02/16 Pct Recovery = 85% Analysis Date = 01/02/16 Pct Recovery = 85% Analysis Date = 12/29/15 Pct Recovery = 85% Analysis Date = 12/29/15 Pct Recovery = 85% Analysis Date = 12/24/15 Pct Recovery = 85% Analysis Date = 12/24/15 Pct Recovery = 85% Analysis Date = 12/19/15 Pct Recovery = 85% Analysis Date = 12/19/15 Pct Recovery = 85% Analysis Date = 12/14/15 Pct Recovery = 85% Analysis Date = 12/14/15 Pct Recovery = 85% Analysis Date = 12/09/15 Pct Recovery = 85% Analysis Date = 12/09/15 Pct Recovery = 85% Analysis Date = 12/05/15 Pct Recovery = 85% Analysis Date = 12/05/15 Pct Recovery = 85% Analysis Date = 11/30/15 Pct Recovery = 85% Analysis Date = 11/30/15 Pct Recovery = 85% Analysis Date = 11/25/15 Pct Recovery = 85% Analysis Date = 11/25/15 Pct Recovery = 85% Analysis Date = 11/20/15 Pct Recovery = 85% Analysis Date = 11/20/15 Pct Recovery = 85% Analysis Date = 11/16/15 Pct Recovery = 85% Analysis Date = 11/16/15 Pct Recovery = 85% Analysis Date = 11/11/15 Pct Recovery = 85% Analysis Date = 11/11/15 Pct Recovery = 85% Analysis Date = 11/06/15 Pct Recovery = 85% Analysis Date = 11/06/15 Pct Recovery = 85% Analysis Date = 11/01/15 Pct Recovery = 85% Analysis Date = 11/01/15 Pct Recovery = 85% Analysis Date = 10/27/15 Pct Recovery = 85% Analysis Date = 10/27/15 Pct Recovery = 85% Analysis Date = 10/23/15 Pct Recovery = 86% Analysis Date = 10/23/15 Pct Recovery = 86% Analysis Date = 10/18/15 Pct Recovery = 86% Analysis Date = 10/18/15 Pct Recovery = 86% Analysis Date = 10/13/15 Pct Recovery = 86% Analysis Date = 10/13/15 Pct Recovery = 86% Analysis Date = 10/08/15 Pct Recovery = 85% Analysis Date = 10/08/15 Pct Recovery = 85% Analysis Date = 10/04/15 Pct Recovery = 85% Analysis Date = 10/04/15 Pct Recovery = 85% Analysis Date = 09/29/15 Pct Recovery = 85% Analysis Date = 09/29/15 Pct Recovery = 85% Analysis Date = 09/24/15 Pct Recovery = 85% Analysis Date = 09/24/15 Pct Recovery = 85% Analysis Date = 09/19/15 Pct Recovery = 85% Analysis Date = 09/19/15 Pct Recovery = 85% Analysis Date = 09/14/15 Pct Recovery = 85% Analysis Date = 09/14/15 Pct Recovery = 85% Analysis Date = 09/10/15 Pct Recovery = 85% Analysis Date = 09/10/15 Pct Recovery = 85% Analysis Date = 09/05/15 Pct Recovery = 85% Analysis Date = 09/05/15 Pct Recovery = 85% Analysis Date = 08/31/15 Pct Recovery = 85% Analysis Date = 08/31/15 Pct Recovery = 85% Analysis Date = 08/26/15 Pct Recovery = 85% Analysis Date = 08/26/15 Pct Recovery = 85% Analysis Date = 08/21/15 Pct Recovery = 85% Analysis Date = 08/21/15 Pct Recovery = 85% Analysis Date = 08/17/15 Pct Recovery = 85% Analysis Date = 08/17/15 Pct Recovery = 85% Analysis Date = 08/12/15 Pct Recovery = 85% Analysis Date = 08/12/15 Pct Recovery = 85% Analysis Date = 08/07/15 Pct Recovery = 85% Analysis Date = 08/07/15 Pct Recovery = 85% Analysis Date = 08/02/15 Pct Recovery = 85% Analysis Date = 08/02/15 Pct Recovery = 85% Analysis Date = 07/29/15 Pct Recovery = 85% Analysis Date = 07/29/15 Pct Recovery = 85% Analysis Date = 07/24/15 Pct Recovery = 85% Analysis Date = 07/24/15 Pct Recovery = 85% Analysis Date = 07/19/15 Pct Recovery = 85% Analysis Date = 07/19/15 Pct Recovery = 85% Analysis Date = 07/14/15 Pct Recovery = 84% Analysis Date = 07/14/15 Pct Recovery = 84% Analysis Date = 07/09/15 Pct Recovery = 84% Analysis Date = 07/09/15 Pct Recovery = 84% Analysis Date = 07/05/15 Pct Recovery = 84% Analysis Date = 07/05/15 Pct Recovery = 84% Analysis Date = 06/30/15 Pct Recovery = 84% Analysis Date = 06/30/15 Pct Recovery = 84% Analysis Date = 06/25/15 Pct Recovery = 84% Analysis Date = 06/25/15 Pct Recovery = 84% Analysis Date = 06/20/15 Pct Recovery = 84% Analysis Date = 06/20/15 Pct Recovery = 84% Analysis Date = 06/16/15 Pct Recovery = 84% Analysis Date = 06/16/15 Pct Recovery = 84% Analysis Date = 06/11/15 Pct Recovery = 84% Analysis Date = 06/11/15 Pct Recovery = 84% Analysis Date = 06/06/15 Pct Recovery = 84% Analysis Date = 06/06/15 Pct Recovery = 84% Analysis Date = 06/01/15 Pct Recovery = 84% Analysis Date = 06/01/15 Pct Recovery = 84% Analysis Date = 05/27/15 Pct Recovery = 84% Analysis Date = 05/27/15 Pct Recovery = 84% Analysis Date = 05/23/15 Pct Recovery = 84% Analysis Date = 05/23/15 Pct Recovery = 84% Analysis Date = 05/18/15 Pct Recovery = 84% Analysis Date = 05/18/15 Pct Recovery = 84% Analysis Date = 05/13/15 Pct Recovery = 84% Analysis Date = 05/13/15 Pct Recovery = 84% Analysis Date = 05/08/15 Pct Recovery = 84% Analysis Date = 05/08/15 Pct Recovery = 84% Analysis Date = 05/04/15 Pct Recovery = 84% Analysis Date = 05/04/15 Pct Recovery = 84% Analysis Date = 04/29/15 Pct Recovery = 84% Analysis Date = 04/29/15 Pct Recovery = 84% Analysis Date = 04/24/15 Pct Recovery = 84% Analysis Date = 04/24/15 Pct Recovery = 84% Analysis Date = 04/19/15 Pct Recovery = 83% Analysis Date = 04/19/15 Pct Recovery = 83% Analysis Date = 04/14/15 Pct Recovery = 83% Analysis Date = 04/14/15 Pct Recovery = 83% Analysis Date = 04/10/15 Pct Recovery = 83% Analysis Date = 04/10/15 Pct Recovery = 83% Analysis Date = 04/05/15 Pct Recovery = 83% Analysis Date = 04/05/15 Pct Recovery = 83% Analysis Date = 03/31/15 Pct Recovery = 83% Analysis Date = 03/31/15 Pct Recovery = 83% Analysis Date = 03/26/15 Pct Recovery = 83% Analysis Date = 03/26/15 Pct Recovery = 83% Analysis Date = 03/22/15 Pct Recovery = 83% Analysis Date = 03/22/15 Pct Recovery = 83% Analysis Date = 03/17/15 Pct Recovery = 83% Analysis Date = 03/17/15 Pct Recovery = 83% Analysis Date = 03/12/15 Pct Recovery = 83% Analysis Date = 03/12/15 Pct Recovery = 83% Analysis Date = 03/07/15 Pct Recovery = 83% Analysis Date = 03/07/15 Pct Recovery = 83% Analysis Date = 03/02/15 Pct Recovery = 83% Analysis Date = 03/02/15 Pct Recovery = 83% Analysis Date = 02/26/15 Pct Recovery = 83% Analysis Date = 02/26/15 Pct Recovery = 83% Analysis Date = 02/21/15 Pct Recovery = 83% Analysis Date = 02/21/15 Pct Recovery = 83% Analysis Date = 02/16/15 Pct Recovery = 83% Analysis Date = 02/16/15 Pct Recovery = 83% Analysis Date = 02/11/15 Pct Recovery = 83% Analysis Date = 02/11/15 Pct Recovery = 83% Analysis Date = 02/07/15 Pct Recovery = 83% Analysis Date = 02/07/15 Pct Recovery = 83% Analysis Date = 02/02/15 Pct Recovery = 83% Analysis Date = 02/02/15 Pct Recovery = 83% Analysis Date = 01/28/15 Pct Recovery = 83% Analysis Date = 01/28/15 Pct Recovery = 83% Analysis Date = 01/23/15 Pct Recovery = 83% Analysis Date = 01/23/15 Pct Recovery = 83% Analysis Date = 01/18/15 Pct Recovery = 83% Analysis Date = 01/18/15 Pct Recovery = 83% Analysis Date = 01/14/15 Pct Recovery = 83% Analysis Date = 01/14/15 Pct Recovery = 83% Analysis Date = 01/09/15 Pct Recovery = 83% Analysis Date = 01/09/15 Pct Recovery = 83% Analysis Date = 01/04/15 Pct Recovery = 83% Analysis Date = 01/04/15 Pct Recovery = 83% Analysis Date = 12/30/14 Pct Recovery = 83% Analysis Date = 12/30/14 Pct Recovery = 83% Analysis Date = 12/25/14 Pct Recovery = 82% Analysis Date = 12/25/14 Pct Recovery = 82% Analysis Date = 12/21/14 Pct Recovery = 82% Analysis Date = 12/21/14 Pct Recovery = 82% Analysis Date = 12/16/14 Pct Recovery = 82% Analysis Date = 12/16/14 Pct Recovery = 82% Analysis Date = 12/11/14 Pct Recovery = 82% Analysis Date = 12/11/14 Pct Recovery = 82% Analysis Date = 12/06/14 Pct Recovery = 82% Analysis Date = 12/06/14 Pct Recovery = 82% Analysis Date = 12/02/14 Pct Recovery = 82% Analysis Date = 12/02/14 Pct Recovery = 82% Analysis Date = 11/27/14 Pct Recovery = 82% Analysis Date = 11/27/14 Pct Recovery = 82% Analysis Date = 11/22/14 Pct Recovery = 82% Analysis Date = 11/22/14 Pct Recovery = 82% Analysis Date = 11/17/14 Pct Recovery = 82% Analysis Date = 11/17/14 Pct Recovery = 82% Analysis Date = 11/12/14 Pct Recovery = 82% Analysis Date = 11/12/14 Pct Recovery = 82% Analysis Date = 11/08/14 Pct Recovery = 82% Analysis Date = 11/08/14 Pct Recovery = 82% Analysis Date = 11/03/14 Pct Recovery = 82% Analysis Date = 11/03/14 Pct Recovery = 82% Analysis Date = 10/29/14 Pct Recovery = 82% Analysis Date = 10/29/14 Pct Recovery = 82% Analysis Date = 10/24/14 Pct Recovery = 82% Analysis Date = 10/24/14 Pct Recovery = 82% Analysis Date = 10/20/14 Pct Recovery = 82% Analysis Date = 10/20/14 Pct Recovery = 82% Analysis Date = 10/15/14 Pct Recovery = 82% Analysis Date = 10/15/14 Pct Recovery = 82% Analysis Date = 10/10/14 Pct Recovery = 82% Analysis Date = 10/10/14 Pct Recovery = 82% Analysis Date = 10/05/14 Pct Recovery = 82% Analysis Date = 10/05/14 Pct Recovery = 82% Analysis Date = 09/30/14 Pct Recovery = 82% Analysis Date = 09/30/14 Pct Recovery = 82% Analysis Date = 09/26/14 Pct Recovery = 81% Analysis Date = 09/26/14 Pct Recovery = 81% Analysis Date = 09/21/14 Pct Recovery = 81% Analysis Date = 09/21/14 Pct Recovery = 81% Analysis Date = 09/16/14 Pct Recovery = 81% Analysis Date = 09/16/14 Pct Recovery = 81% Analysis Date = 09/11/14 Pct Recovery = 81% Analysis Date = 09/11/14 Pct Recovery = 81% Analysis Date = 09/07/14 Pct Recovery = 81% Analysis Date = 09/07/14 Pct Recovery = 81% Analysis Date = 09/02/14 Pct Recovery = 81% Analysis Date = 09/02/14 Pct Recovery = 81% Analysis Date = 08/28/14 Pct Recovery = 81% Analysis Date = 08/28/14 Pct Recovery = 81% Analysis Date = 08/23/14 Pct Recovery = 81% Analysis Date = 08/23/14 Pct Recovery = 81% Analysis Date = 08/18/14 Pct Recovery = 81% Analysis Date = 08/18/14 Pct Recovery = 81% Analysis Date = 08/14/14 Pct Recovery = 81% Analysis Date = 08/14/14 Pct Recovery = 81% Analysis Date = 08/09/14 Pct Recovery = 81% Analysis Date = 08/09/14 Pct Recovery = 81% Analysis Date = 08/04/14 Pct Recovery = 81% Analysis Date = 08/04/14 Pct Recovery = 81% Analysis Date = 07/30/14 Pct Recovery = 81% Analysis Date = 07/30/14 Pct Recovery = 81% Analysis Date = 07/26/14 Pct Recovery = 81% Analysis Date = 07/26/14 Pct Recovery = 81% Analysis Date = 07/21/14 Pct Recovery = 81% Analysis Date = 07/21/14 Pct Recovery = 81% Analysis Date = 07/16/14 Pct Recovery = 81% Analysis Date = 07/16/14 Pct Recovery = 81% Analysis Date = 07/11/14 Pct Recovery = 81% Analysis Date = 07/11/14 Pct Recovery = 81% Analysis Date = 07/06/14 Pct Recovery = 81% Analysis Date = 07/06/14 Pct Recovery = 81% Analysis Date = 07/02/14 Pct Recovery = 80% Analysis Date = 07/02/14 Pct Recovery = 80% Analysis Date = 06/27/14 Pct Recovery = 80% Analysis Date = 06/27/14 Pct Recovery = 80% Analysis Date = 06/22/14 Pct Recovery = 80% Analysis Date = 06/22/14 Pct Recovery = 80% Analysis Date = 06/17/14 Pct Recovery = 80% Analysis Date = 06/17/14 Pct Recovery = 80% Analysis Date = 06/13/14 Pct Recovery = 80% Analysis Date = 06/13/14 Pct Recovery = 80% Analysis Date = 06/08/14 Pct Recovery = 80% Analysis Date = 06/08/14 Pct Recovery = 80% Analysis Date = 06/03/14 Pct Recovery = 80% Analysis Date = 06/03/14 Pct Recovery = 80% Analysis Date = 05/29/14 Pct Recovery = 80% Analysis Date = 05/29/14 Pct Recovery = 80% Analysis Date = 05/24/14 Pct Recovery = 80% Analysis Date = 05/24/14 Pct Recovery = 80% Analysis Date = 05/20/14 Pct Recovery = 80% Analysis Date = 05/20/14 Pct Recovery = 80% Analysis Date = 05/15/14 Pct Recovery = 80% Analysis Date = 05/15/14 Pct Recovery = 80% Analysis Date = 05/10/14 Pct Recovery = 80% Analysis Date = 05/10/14 Pct Recovery = 80% Analysis Date = 05/05/14 Pct Recovery = 80% Analysis Date = 05/05/14 Pct Recovery = 80% Analysis Date = 05/01/14 Pct Recovery = 80% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
TERT-BUTYLBENZENE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 48 84% 8% 84% 8%
Total 48 84% 8% 84% 8%

Sample Statistics
TERT-BUTYLBENZENE

Characteristic N % % Basis
Plotted 48 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 48 .  
False Negatives 0 0% 0 out of 48
Not Spiked 25 .  
False Positives 0 0% 0 out of 25

BQS OBSP Determination:
TERT-BUTYL METHYL ETHER (MTBE)
METHOD: 4440 , TESTIDCODE: 78032GCM66
Open Data Set

Analysis Date = 12/16/16 SpikeMix = NSI 041816AVOC: 40 µl & ChemService 5082900: 40 µl Pct Recovery = 100% Analysis Date = 08/04/16 SpikeMix = Crescent 03FF058: 40 µl & Supelco LC20141V: 40 µl Pct Recovery = 87% Analysis Date = 07/20/16 SpikeMix = Supelco LC20141V: 40 µl & Accu 216041125: 40 µl Pct Recovery = 103% Analysis Date = 08/31/16 SpikeMix = NSI 041816AVOC: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 98% Analysis Date = 08/12/16 SpikeMix = ChemService 5082900: 25 µl & Phenova B20160319: 25 µl Pct Recovery = 107% Analysis Date = 06/30/16 SpikeMix = Crescent 03FF058: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 106% Analysis Date = 11/21/16 SpikeMix = Crescent 03FF058: 25 µl & Supelco LC20141V: 25 µl Pct Recovery = 101% Analysis Date = 09/08/16 SpikeMix = Supelco LC20141V: 25 µl & Accu 216041125: 25 µl Pct Recovery = 102% Analysis Date = 03/06/15 SpikeMix = ERA 0227-14-06.1A: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 103% Analysis Date = 12/17/14 SpikeMix = Supelco LC06438: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 104% Analysis Date = 09/21/14 SpikeMix = Supelco LC06438: 20 µl Pct Recovery = 122% Analysis Date = 06/10/14 SpikeMix = NSI 032614: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 104% Analysis Date = 03/19/15 SpikeMix = Spex Organics C1140417015: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 110% Analysis Date = 11/22/14 SpikeMix = NSI 032614: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 110% Analysis Date = 08/19/14 SpikeMix = Spex Organics C1140417015: 20 µl & Accu 214031115: 20 µl Pct Recovery = 107% Analysis Date = 08/16/14 SpikeMix = ERA 0227-14-06.1A: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 102% Analysis Date = 09/29/15 SpikeMix = Accu 215041380: 25 µl & ERA 0406-15-03: 25 µl Pct Recovery = 87% Analysis Date = 08/15/15 SpikeMix = Supelco LC13545: 25 µl & Crescent 04EE008: 25 µl Pct Recovery = 85% Analysis Date = 07/13/15 SpikeMix = Crescent 04EE008: 25 µl & NSI 050515AVOC: 25 µl Pct Recovery = 101% Analysis Date = 11/29/16 SpikeMix = ChemService 5082900: 15 µl & Phenova B20160319: 15 µl Pct Recovery = 108% Analysis Date = 09/28/16 SpikeMix = Crescent 03FF058: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 105% Analysis Date = 06/30/16 SpikeMix = ChemService 5082900: 15 µl & Accu 216041125: 15 µl Pct Recovery = 116% Analysis Date = 06/10/16 SpikeMix = NSI 041816AVOC: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 96% Analysis Date = 10/13/16 SpikeMix = NSI 041816AVOC: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 121% Analysis Date = 05/27/16 SpikeMix = Phenova B20160319: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 104% Analysis Date = 04/02/16 SpikeMix = Supelco LC13545: 15 µl & Accu 215041380: 15 µl Pct Recovery = 99% Analysis Date = 03/04/16 SpikeMix = Accu 215041380: 15 µl & ERA 0406-15-03: 15 µl Pct Recovery = 95% Analysis Date = 06/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Accu 215041380: 15 µl Pct Recovery = 89% Analysis Date = 12/18/15 SpikeMix = Supelco LC13545: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 92% Analysis Date = 10/17/15 SpikeMix = Crescent 04EE008: 15 µl & NSI 050515AVOC: 15 µl Pct Recovery = 88% Analysis Date = 05/09/15 SpikeMix = Spex Organics EN150428007: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 95% Analysis Date = 10/21/14 SpikeMix = ERA 0227-14-06.1A: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 110% Analysis Date = 06/18/14 SpikeMix = Supelco LC06438: 10 µl & Accu 214031115: 10 µl Pct Recovery = 110% Analysis Date = 05/30/14 SpikeMix = NSI 032614: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 92% Analysis Date = 05/03/14 SpikeMix = Crescent 03DD004: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 101% Analysis Date = 11/06/14 SpikeMix = Spex Organics C1140417015: 10 µl & Crescent 03DD004: 10 µl Pct Recovery = 114% Analysis Date = 09/09/14 SpikeMix = NSI 032614: 10 µl & Spex Organics C1140417015: 10 µl Pct Recovery = 120% Analysis Date = 07/23/14 SpikeMix = Spex Organics C1140417015: 10 µl & Accu 214031115: 10 µl Pct Recovery = 110% Analysis Date = 07/11/14 SpikeMix = Spex Organics C1140417015: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 111% Analysis Date = 02/18/16 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 94% Analysis Date = 11/20/15 SpikeMix = Accu 215041380: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 91% Analysis Date = 11/12/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 94% Analysis Date = 05/21/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 104% Analysis Date = 05/13/16 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 102% Analysis Date = 01/27/16 SpikeMix = Crescent 04EE008: 10 µl & NSI 050515AVOC: 10 µl Pct Recovery = 90% Analysis Date = 08/07/15 SpikeMix = Crescent 04EE008: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 103% Analysis Date = 05/09/15 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 91% Analysis Date = 12/16/16 Pct Recovery = 107% Analysis Date = 12/11/16 Pct Recovery = 107% Analysis Date = 12/11/16 Pct Recovery = 107% Analysis Date = 12/06/16 Pct Recovery = 107% Analysis Date = 12/06/16 Pct Recovery = 107% Analysis Date = 12/01/16 Pct Recovery = 107% Analysis Date = 12/01/16 Pct Recovery = 107% Analysis Date = 11/26/16 Pct Recovery = 107% Analysis Date = 11/26/16 Pct Recovery = 107% Analysis Date = 11/22/16 Pct Recovery = 107% Analysis Date = 11/22/16 Pct Recovery = 107% Analysis Date = 11/17/16 Pct Recovery = 106% Analysis Date = 11/17/16 Pct Recovery = 106% Analysis Date = 11/12/16 Pct Recovery = 106% Analysis Date = 11/12/16 Pct Recovery = 106% Analysis Date = 11/07/16 Pct Recovery = 106% Analysis Date = 11/07/16 Pct Recovery = 106% Analysis Date = 11/02/16 Pct Recovery = 106% Analysis Date = 11/02/16 Pct Recovery = 106% Analysis Date = 10/29/16 Pct Recovery = 106% Analysis Date = 10/29/16 Pct Recovery = 106% Analysis Date = 10/24/16 Pct Recovery = 106% Analysis Date = 10/24/16 Pct Recovery = 106% Analysis Date = 10/19/16 Pct Recovery = 105% Analysis Date = 10/19/16 Pct Recovery = 105% Analysis Date = 10/14/16 Pct Recovery = 105% Analysis Date = 10/14/16 Pct Recovery = 105% Analysis Date = 10/09/16 Pct Recovery = 105% Analysis Date = 10/09/16 Pct Recovery = 105% Analysis Date = 10/05/16 Pct Recovery = 105% Analysis Date = 10/05/16 Pct Recovery = 105% Analysis Date = 09/30/16 Pct Recovery = 105% Analysis Date = 09/30/16 Pct Recovery = 105% Analysis Date = 09/25/16 Pct Recovery = 104% Analysis Date = 09/25/16 Pct Recovery = 104% Analysis Date = 09/20/16 Pct Recovery = 104% Analysis Date = 09/20/16 Pct Recovery = 104% Analysis Date = 09/15/16 Pct Recovery = 104% Analysis Date = 09/15/16 Pct Recovery = 104% Analysis Date = 09/11/16 Pct Recovery = 104% Analysis Date = 09/11/16 Pct Recovery = 104% Analysis Date = 09/06/16 Pct Recovery = 104% Analysis Date = 09/06/16 Pct Recovery = 104% Analysis Date = 09/01/16 Pct Recovery = 104% Analysis Date = 09/01/16 Pct Recovery = 104% Analysis Date = 08/27/16 Pct Recovery = 103% Analysis Date = 08/27/16 Pct Recovery = 103% Analysis Date = 08/23/16 Pct Recovery = 103% Analysis Date = 08/23/16 Pct Recovery = 103% Analysis Date = 08/18/16 Pct Recovery = 103% Analysis Date = 08/18/16 Pct Recovery = 103% Analysis Date = 08/13/16 Pct Recovery = 103% Analysis Date = 08/13/16 Pct Recovery = 103% Analysis Date = 08/08/16 Pct Recovery = 103% Analysis Date = 08/08/16 Pct Recovery = 103% Analysis Date = 08/03/16 Pct Recovery = 103% Analysis Date = 08/03/16 Pct Recovery = 103% Analysis Date = 07/30/16 Pct Recovery = 102% Analysis Date = 07/30/16 Pct Recovery = 102% Analysis Date = 07/25/16 Pct Recovery = 102% Analysis Date = 07/25/16 Pct Recovery = 102% Analysis Date = 07/20/16 Pct Recovery = 102% Analysis Date = 07/20/16 Pct Recovery = 102% Analysis Date = 07/15/16 Pct Recovery = 102% Analysis Date = 07/15/16 Pct Recovery = 102% Analysis Date = 07/10/16 Pct Recovery = 102% Analysis Date = 07/10/16 Pct Recovery = 102% Analysis Date = 07/06/16 Pct Recovery = 101% Analysis Date = 07/06/16 Pct Recovery = 101% Analysis Date = 07/01/16 Pct Recovery = 101% Analysis Date = 07/01/16 Pct Recovery = 101% Analysis Date = 06/26/16 Pct Recovery = 101% Analysis Date = 06/26/16 Pct Recovery = 101% Analysis Date = 06/21/16 Pct Recovery = 101% Analysis Date = 06/21/16 Pct Recovery = 101% Analysis Date = 06/16/16 Pct Recovery = 101% Analysis Date = 06/16/16 Pct Recovery = 101% Analysis Date = 06/12/16 Pct Recovery = 101% Analysis Date = 06/12/16 Pct Recovery = 101% Analysis Date = 06/07/16 Pct Recovery = 100% Analysis Date = 06/07/16 Pct Recovery = 100% Analysis Date = 06/02/16 Pct Recovery = 100% Analysis Date = 06/02/16 Pct Recovery = 100% Analysis Date = 05/28/16 Pct Recovery = 100% Analysis Date = 05/28/16 Pct Recovery = 100% Analysis Date = 05/24/16 Pct Recovery = 100% Analysis Date = 05/24/16 Pct Recovery = 100% Analysis Date = 05/19/16 Pct Recovery = 100% Analysis Date = 05/19/16 Pct Recovery = 100% Analysis Date = 05/14/16 Pct Recovery = 99% Analysis Date = 05/14/16 Pct Recovery = 99% Analysis Date = 05/09/16 Pct Recovery = 99% Analysis Date = 05/09/16 Pct Recovery = 99% Analysis Date = 05/04/16 Pct Recovery = 99% Analysis Date = 05/04/16 Pct Recovery = 99% Analysis Date = 04/30/16 Pct Recovery = 99% Analysis Date = 04/30/16 Pct Recovery = 99% Analysis Date = 04/25/16 Pct Recovery = 99% Analysis Date = 04/25/16 Pct Recovery = 99% Analysis Date = 04/20/16 Pct Recovery = 99% Analysis Date = 04/20/16 Pct Recovery = 99% Analysis Date = 04/15/16 Pct Recovery = 98% Analysis Date = 04/15/16 Pct Recovery = 98% Analysis Date = 04/10/16 Pct Recovery = 98% Analysis Date = 04/10/16 Pct Recovery = 98% Analysis Date = 04/06/16 Pct Recovery = 98% Analysis Date = 04/06/16 Pct Recovery = 98% Analysis Date = 04/01/16 Pct Recovery = 98% Analysis Date = 04/01/16 Pct Recovery = 98% Analysis Date = 03/27/16 Pct Recovery = 98% Analysis Date = 03/27/16 Pct Recovery = 98% Analysis Date = 03/22/16 Pct Recovery = 97% Analysis Date = 03/22/16 Pct Recovery = 97% Analysis Date = 03/17/16 Pct Recovery = 97% Analysis Date = 03/17/16 Pct Recovery = 97% Analysis Date = 03/13/16 Pct Recovery = 97% Analysis Date = 03/13/16 Pct Recovery = 97% Analysis Date = 03/08/16 Pct Recovery = 97% Analysis Date = 03/08/16 Pct Recovery = 97% Analysis Date = 03/03/16 Pct Recovery = 97% Analysis Date = 03/03/16 Pct Recovery = 97% Analysis Date = 02/27/16 Pct Recovery = 96% Analysis Date = 02/27/16 Pct Recovery = 96% Analysis Date = 02/23/16 Pct Recovery = 96% Analysis Date = 02/23/16 Pct Recovery = 96% Analysis Date = 02/18/16 Pct Recovery = 96% Analysis Date = 02/18/16 Pct Recovery = 96% Analysis Date = 02/13/16 Pct Recovery = 96% Analysis Date = 02/13/16 Pct Recovery = 96% Analysis Date = 02/08/16 Pct Recovery = 96% Analysis Date = 02/08/16 Pct Recovery = 96% Analysis Date = 02/03/16 Pct Recovery = 96% Analysis Date = 02/03/16 Pct Recovery = 96% Analysis Date = 01/30/16 Pct Recovery = 96% Analysis Date = 01/30/16 Pct Recovery = 96% Analysis Date = 01/25/16 Pct Recovery = 96% Analysis Date = 01/25/16 Pct Recovery = 96% Analysis Date = 01/20/16 Pct Recovery = 96% Analysis Date = 01/20/16 Pct Recovery = 96% Analysis Date = 01/15/16 Pct Recovery = 95% Analysis Date = 01/15/16 Pct Recovery = 95% Analysis Date = 01/10/16 Pct Recovery = 95% Analysis Date = 01/10/16 Pct Recovery = 95% Analysis Date = 01/06/16 Pct Recovery = 95% Analysis Date = 01/06/16 Pct Recovery = 95% Analysis Date = 01/01/16 Pct Recovery = 95% Analysis Date = 01/01/16 Pct Recovery = 95% Analysis Date = 12/27/15 Pct Recovery = 95% Analysis Date = 12/27/15 Pct Recovery = 95% Analysis Date = 12/22/15 Pct Recovery = 95% Analysis Date = 12/22/15 Pct Recovery = 95% Analysis Date = 12/17/15 Pct Recovery = 95% Analysis Date = 12/17/15 Pct Recovery = 95% Analysis Date = 12/13/15 Pct Recovery = 95% Analysis Date = 12/13/15 Pct Recovery = 95% Analysis Date = 12/08/15 Pct Recovery = 95% Analysis Date = 12/08/15 Pct Recovery = 95% Analysis Date = 12/03/15 Pct Recovery = 95% Analysis Date = 12/03/15 Pct Recovery = 95% Analysis Date = 11/28/15 Pct Recovery = 95% Analysis Date = 11/28/15 Pct Recovery = 95% Analysis Date = 11/24/15 Pct Recovery = 94% Analysis Date = 11/24/15 Pct Recovery = 94% Analysis Date = 11/19/15 Pct Recovery = 94% Analysis Date = 11/19/15 Pct Recovery = 94% Analysis Date = 11/14/15 Pct Recovery = 94% Analysis Date = 11/14/15 Pct Recovery = 94% Analysis Date = 11/09/15 Pct Recovery = 94% Analysis Date = 11/09/15 Pct Recovery = 94% Analysis Date = 11/04/15 Pct Recovery = 94% Analysis Date = 11/04/15 Pct Recovery = 94% Analysis Date = 10/31/15 Pct Recovery = 94% Analysis Date = 10/31/15 Pct Recovery = 94% Analysis Date = 10/26/15 Pct Recovery = 94% Analysis Date = 10/26/15 Pct Recovery = 94% Analysis Date = 10/21/15 Pct Recovery = 94% Analysis Date = 10/21/15 Pct Recovery = 94% Analysis Date = 10/16/15 Pct Recovery = 94% Analysis Date = 10/16/15 Pct Recovery = 94% Analysis Date = 10/11/15 Pct Recovery = 94% Analysis Date = 10/11/15 Pct Recovery = 94% Analysis Date = 10/07/15 Pct Recovery = 94% Analysis Date = 10/07/15 Pct Recovery = 94% Analysis Date = 10/02/15 Pct Recovery = 95% Analysis Date = 10/02/15 Pct Recovery = 95% Analysis Date = 09/27/15 Pct Recovery = 95% Analysis Date = 09/27/15 Pct Recovery = 95% Analysis Date = 09/22/15 Pct Recovery = 95% Analysis Date = 09/22/15 Pct Recovery = 95% Analysis Date = 09/17/15 Pct Recovery = 95% Analysis Date = 09/17/15 Pct Recovery = 95% Analysis Date = 09/13/15 Pct Recovery = 95% Analysis Date = 09/13/15 Pct Recovery = 95% Analysis Date = 09/08/15 Pct Recovery = 95% Analysis Date = 09/08/15 Pct Recovery = 95% Analysis Date = 09/03/15 Pct Recovery = 95% Analysis Date = 09/03/15 Pct Recovery = 95% Analysis Date = 08/29/15 Pct Recovery = 95% Analysis Date = 08/29/15 Pct Recovery = 95% Analysis Date = 08/25/15 Pct Recovery = 95% Analysis Date = 08/25/15 Pct Recovery = 95% Analysis Date = 08/20/15 Pct Recovery = 95% Analysis Date = 08/20/15 Pct Recovery = 95% Analysis Date = 08/15/15 Pct Recovery = 96% Analysis Date = 08/15/15 Pct Recovery = 96% Analysis Date = 08/10/15 Pct Recovery = 96% Analysis Date = 08/10/15 Pct Recovery = 96% Analysis Date = 08/05/15 Pct Recovery = 96% Analysis Date = 08/05/15 Pct Recovery = 96% Analysis Date = 08/01/15 Pct Recovery = 96% Analysis Date = 08/01/15 Pct Recovery = 96% Analysis Date = 07/27/15 Pct Recovery = 96% Analysis Date = 07/27/15 Pct Recovery = 96% Analysis Date = 07/22/15 Pct Recovery = 96% Analysis Date = 07/22/15 Pct Recovery = 96% Analysis Date = 07/17/15 Pct Recovery = 96% Analysis Date = 07/17/15 Pct Recovery = 96% Analysis Date = 07/12/15 Pct Recovery = 96% Analysis Date = 07/12/15 Pct Recovery = 96% Analysis Date = 07/08/15 Pct Recovery = 97% Analysis Date = 07/08/15 Pct Recovery = 97% Analysis Date = 07/03/15 Pct Recovery = 97% Analysis Date = 07/03/15 Pct Recovery = 97% Analysis Date = 06/28/15 Pct Recovery = 97% Analysis Date = 06/28/15 Pct Recovery = 97% Analysis Date = 06/23/15 Pct Recovery = 97% Analysis Date = 06/23/15 Pct Recovery = 97% Analysis Date = 06/18/15 Pct Recovery = 97% Analysis Date = 06/18/15 Pct Recovery = 97% Analysis Date = 06/14/15 Pct Recovery = 98% Analysis Date = 06/14/15 Pct Recovery = 98% Analysis Date = 06/09/15 Pct Recovery = 98% Analysis Date = 06/09/15 Pct Recovery = 98% Analysis Date = 06/04/15 Pct Recovery = 98% Analysis Date = 06/04/15 Pct Recovery = 98% Analysis Date = 05/30/15 Pct Recovery = 98% Analysis Date = 05/30/15 Pct Recovery = 98% Analysis Date = 05/25/15 Pct Recovery = 99% Analysis Date = 05/25/15 Pct Recovery = 99% Analysis Date = 05/21/15 Pct Recovery = 99% Analysis Date = 05/21/15 Pct Recovery = 99% Analysis Date = 05/16/15 Pct Recovery = 99% Analysis Date = 05/16/15 Pct Recovery = 99% Analysis Date = 05/11/15 Pct Recovery = 99% Analysis Date = 05/11/15 Pct Recovery = 99% Analysis Date = 05/06/15 Pct Recovery = 100% Analysis Date = 05/06/15 Pct Recovery = 100% Analysis Date = 05/02/15 Pct Recovery = 100% Analysis Date = 05/02/15 Pct Recovery = 100% Analysis Date = 04/27/15 Pct Recovery = 100% Analysis Date = 04/27/15 Pct Recovery = 100% Analysis Date = 04/22/15 Pct Recovery = 100% Analysis Date = 04/22/15 Pct Recovery = 100% Analysis Date = 04/17/15 Pct Recovery = 100% Analysis Date = 04/17/15 Pct Recovery = 100% Analysis Date = 04/12/15 Pct Recovery = 101% Analysis Date = 04/12/15 Pct Recovery = 101% Analysis Date = 04/08/15 Pct Recovery = 101% Analysis Date = 04/08/15 Pct Recovery = 101% Analysis Date = 04/03/15 Pct Recovery = 101% Analysis Date = 04/03/15 Pct Recovery = 101% Analysis Date = 03/29/15 Pct Recovery = 101% Analysis Date = 03/29/15 Pct Recovery = 101% Analysis Date = 03/24/15 Pct Recovery = 102% Analysis Date = 03/24/15 Pct Recovery = 102% Analysis Date = 03/19/15 Pct Recovery = 102% Analysis Date = 03/19/15 Pct Recovery = 102% Analysis Date = 03/15/15 Pct Recovery = 102% Analysis Date = 03/15/15 Pct Recovery = 102% Analysis Date = 03/10/15 Pct Recovery = 102% Analysis Date = 03/10/15 Pct Recovery = 102% Analysis Date = 03/05/15 Pct Recovery = 103% Analysis Date = 03/05/15 Pct Recovery = 103% Analysis Date = 02/28/15 Pct Recovery = 103% Analysis Date = 02/28/15 Pct Recovery = 103% Analysis Date = 02/23/15 Pct Recovery = 103% Analysis Date = 02/23/15 Pct Recovery = 103% Analysis Date = 02/19/15 Pct Recovery = 103% Analysis Date = 02/19/15 Pct Recovery = 103% Analysis Date = 02/14/15 Pct Recovery = 103% Analysis Date = 02/14/15 Pct Recovery = 103% Analysis Date = 02/09/15 Pct Recovery = 103% Analysis Date = 02/09/15 Pct Recovery = 103% Analysis Date = 02/04/15 Pct Recovery = 103% Analysis Date = 02/04/15 Pct Recovery = 103% Analysis Date = 01/31/15 Pct Recovery = 104% Analysis Date = 01/31/15 Pct Recovery = 104% Analysis Date = 01/26/15 Pct Recovery = 104% Analysis Date = 01/26/15 Pct Recovery = 104% Analysis Date = 01/21/15 Pct Recovery = 104% Analysis Date = 01/21/15 Pct Recovery = 104% Analysis Date = 01/16/15 Pct Recovery = 104% Analysis Date = 01/16/15 Pct Recovery = 104% Analysis Date = 01/11/15 Pct Recovery = 104% Analysis Date = 01/11/15 Pct Recovery = 104% Analysis Date = 01/07/15 Pct Recovery = 104% Analysis Date = 01/07/15 Pct Recovery = 104% Analysis Date = 01/02/15 Pct Recovery = 104% Analysis Date = 01/02/15 Pct Recovery = 104% Analysis Date = 12/28/14 Pct Recovery = 104% Analysis Date = 12/28/14 Pct Recovery = 104% Analysis Date = 12/23/14 Pct Recovery = 105% Analysis Date = 12/23/14 Pct Recovery = 105% Analysis Date = 12/18/14 Pct Recovery = 105% Analysis Date = 12/18/14 Pct Recovery = 105% Analysis Date = 12/14/14 Pct Recovery = 105% Analysis Date = 12/14/14 Pct Recovery = 105% Analysis Date = 12/09/14 Pct Recovery = 105% Analysis Date = 12/09/14 Pct Recovery = 105% Analysis Date = 12/04/14 Pct Recovery = 105% Analysis Date = 12/04/14 Pct Recovery = 105% Analysis Date = 11/29/14 Pct Recovery = 105% Analysis Date = 11/29/14 Pct Recovery = 105% Analysis Date = 11/24/14 Pct Recovery = 105% Analysis Date = 11/24/14 Pct Recovery = 105% Analysis Date = 11/20/14 Pct Recovery = 105% Analysis Date = 11/20/14 Pct Recovery = 105% Analysis Date = 11/15/14 Pct Recovery = 106% Analysis Date = 11/15/14 Pct Recovery = 106% Analysis Date = 11/10/14 Pct Recovery = 106% Analysis Date = 11/10/14 Pct Recovery = 106% Analysis Date = 11/05/14 Pct Recovery = 106% Analysis Date = 11/05/14 Pct Recovery = 106% Analysis Date = 11/01/14 Pct Recovery = 106% Analysis Date = 11/01/14 Pct Recovery = 106% Analysis Date = 10/27/14 Pct Recovery = 106% Analysis Date = 10/27/14 Pct Recovery = 106% Analysis Date = 10/22/14 Pct Recovery = 106% Analysis Date = 10/22/14 Pct Recovery = 106% Analysis Date = 10/17/14 Pct Recovery = 106% Analysis Date = 10/17/14 Pct Recovery = 106% Analysis Date = 10/12/14 Pct Recovery = 106% Analysis Date = 10/12/14 Pct Recovery = 106% Analysis Date = 10/08/14 Pct Recovery = 106% Analysis Date = 10/08/14 Pct Recovery = 106% Analysis Date = 10/03/14 Pct Recovery = 106% Analysis Date = 10/03/14 Pct Recovery = 106% Analysis Date = 09/28/14 Pct Recovery = 107% Analysis Date = 09/28/14 Pct Recovery = 107% Analysis Date = 09/23/14 Pct Recovery = 107% Analysis Date = 09/23/14 Pct Recovery = 107% Analysis Date = 09/18/14 Pct Recovery = 107% Analysis Date = 09/18/14 Pct Recovery = 107% Analysis Date = 09/14/14 Pct Recovery = 107% Analysis Date = 09/14/14 Pct Recovery = 107% Analysis Date = 09/09/14 Pct Recovery = 107% Analysis Date = 09/09/14 Pct Recovery = 107% Analysis Date = 09/04/14 Pct Recovery = 107% Analysis Date = 09/04/14 Pct Recovery = 107% Analysis Date = 08/30/14 Pct Recovery = 107% Analysis Date = 08/30/14 Pct Recovery = 107% Analysis Date = 08/25/14 Pct Recovery = 107% Analysis Date = 08/25/14 Pct Recovery = 107% Analysis Date = 08/21/14 Pct Recovery = 107% Analysis Date = 08/21/14 Pct Recovery = 107% Analysis Date = 08/16/14 Pct Recovery = 107% Analysis Date = 08/16/14 Pct Recovery = 107% Analysis Date = 08/11/14 Pct Recovery = 108% Analysis Date = 08/11/14 Pct Recovery = 108% Analysis Date = 08/06/14 Pct Recovery = 108% Analysis Date = 08/06/14 Pct Recovery = 108% Analysis Date = 08/02/14 Pct Recovery = 108% Analysis Date = 08/02/14 Pct Recovery = 108% Analysis Date = 07/28/14 Pct Recovery = 108% Analysis Date = 07/28/14 Pct Recovery = 108% Analysis Date = 07/23/14 Pct Recovery = 108% Analysis Date = 07/23/14 Pct Recovery = 108% Analysis Date = 07/18/14 Pct Recovery = 108% Analysis Date = 07/18/14 Pct Recovery = 108% Analysis Date = 07/13/14 Pct Recovery = 108% Analysis Date = 07/13/14 Pct Recovery = 108% Analysis Date = 07/09/14 Pct Recovery = 108% Analysis Date = 07/09/14 Pct Recovery = 108% Analysis Date = 07/04/14 Pct Recovery = 108% Analysis Date = 07/04/14 Pct Recovery = 108% Analysis Date = 06/29/14 Pct Recovery = 108% Analysis Date = 06/29/14 Pct Recovery = 108% Analysis Date = 06/24/14 Pct Recovery = 108% Analysis Date = 06/24/14 Pct Recovery = 108% Analysis Date = 06/19/14 Pct Recovery = 108% Analysis Date = 06/19/14 Pct Recovery = 108% Analysis Date = 06/15/14 Pct Recovery = 108% Analysis Date = 06/15/14 Pct Recovery = 108% Analysis Date = 06/10/14 Pct Recovery = 109% Analysis Date = 06/10/14 Pct Recovery = 109% Analysis Date = 06/05/14 Pct Recovery = 109% Analysis Date = 06/05/14 Pct Recovery = 109% Analysis Date = 05/31/14 Pct Recovery = 109% Analysis Date = 05/31/14 Pct Recovery = 109% Analysis Date = 05/26/14 Pct Recovery = 109% Analysis Date = 05/26/14 Pct Recovery = 109% Analysis Date = 05/22/14 Pct Recovery = 109% Analysis Date = 05/22/14 Pct Recovery = 109% Analysis Date = 05/17/14 Pct Recovery = 109% Analysis Date = 05/17/14 Pct Recovery = 109% Analysis Date = 05/12/14 Pct Recovery = 109% Analysis Date = 05/12/14 Pct Recovery = 109% Analysis Date = 05/07/14 Pct Recovery = 109% Analysis Date = 05/07/14 Pct Recovery = 109% Analysis Date = 05/03/14 Pct Recovery = 109% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
TERT-BUTYL METHYL ETHER (MTBE)

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 47 102% 9% 102% 10%
Total 47 102% 9% 102% 10%

Sample Statistics
TERT-BUTYL METHYL ETHER (MTBE)

Characteristic N % % Basis
Plotted 47 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 47 .  
False Negatives 0 0% 0 out of 47
Not Spiked 26 .  
False Positives 2 8% 2 out of 26

BQS OBSP Determination:
TERT-PENTYL METHYL ETHER (TAME)
METHOD: 4440 , TESTIDCODE: 50005GCM66
Open Data Set

Analysis Date = 12/16/16 SpikeMix = NSI 041816AVOC: 40 µl & ChemService 5082900: 40 µl Pct Recovery = 92% Analysis Date = 08/04/16 SpikeMix = Crescent 03FF058: 40 µl & Supelco LC20141V: 40 µl Pct Recovery = 84% Analysis Date = 07/20/16 SpikeMix = Supelco LC20141V: 40 µl & Accu 216041125: 40 µl Pct Recovery = 84% Analysis Date = 08/31/16 SpikeMix = NSI 041816AVOC: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 100% Analysis Date = 08/12/16 SpikeMix = ChemService 5082900: 25 µl & Phenova B20160319: 25 µl Pct Recovery = 103% Analysis Date = 06/30/16 SpikeMix = Crescent 03FF058: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 100% Analysis Date = 11/21/16 SpikeMix = Crescent 03FF058: 25 µl & Supelco LC20141V: 25 µl Pct Recovery = 96% Analysis Date = 09/08/16 SpikeMix = Supelco LC20141V: 25 µl & Accu 216041125: 25 µl Pct Recovery = 92% Analysis Date = 04/09/15 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 99% Analysis Date = 03/06/15 SpikeMix = ERA 0227-14-06.1A: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 98% Analysis Date = 11/22/14 SpikeMix = NSI 032614: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 97% Analysis Date = 11/14/14 SpikeMix = Crescent 03DD004: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 107% Analysis Date = 08/16/14 SpikeMix = ERA 0227-14-06.1A: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 87% Analysis Date = 07/01/14 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 111% Analysis Date = 06/10/14 SpikeMix = Crescent 03DD004: 20 µl & NSI 032614: 20 µl Pct Recovery = 94% Analysis Date = 06/10/14 SpikeMix = NSI 032614: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 102% Analysis Date = 05/01/14 SpikeMix = Accu 214031115: 20 µl & NSI 032614: 20 µl Pct Recovery = 85% Analysis Date = 07/13/15 SpikeMix = Crescent 04EE008: 25 µl & NSI 050515AVOC: 25 µl Pct Recovery = 91% Analysis Date = 09/29/15 SpikeMix = Accu 215041380: 25 µl & ERA 0406-15-03: 25 µl Pct Recovery = 94% Analysis Date = 06/16/15 SpikeMix = ERA 0406-15-03: 25 µl & Supelco LC13545: 25 µl Pct Recovery = 75% Analysis Date = 11/29/16 SpikeMix = ChemService 5082900: 15 µl & Phenova B20160319: 15 µl Pct Recovery = 107% Analysis Date = 09/28/16 SpikeMix = Crescent 03FF058: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 100% Analysis Date = 06/30/16 SpikeMix = ChemService 5082900: 15 µl & Accu 216041125: 15 µl Pct Recovery = 99% Analysis Date = 06/10/16 SpikeMix = NSI 041816AVOC: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 85% Analysis Date = 10/13/16 SpikeMix = NSI 041816AVOC: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 107% Analysis Date = 05/27/16 SpikeMix = Phenova B20160319: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 104% Analysis Date = 11/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 109% Analysis Date = 10/17/15 SpikeMix = Crescent 04EE008: 15 µl & NSI 050515AVOC: 15 µl Pct Recovery = 97% Analysis Date = 06/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Accu 215041380: 15 µl Pct Recovery = 89% Analysis Date = 04/26/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 117% Analysis Date = 03/04/16 SpikeMix = Accu 215041380: 15 µl & ERA 0406-15-03: 15 µl Pct Recovery = 95% Analysis Date = 02/05/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 87% Analysis Date = 10/16/15 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 108% Analysis Date = 01/13/15 SpikeMix = Accu 214031115: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 102% Analysis Date = 10/21/14 SpikeMix = ERA 0227-14-06.1A: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 104% Analysis Date = 10/04/14 SpikeMix = Crescent 03DD004: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 94% Analysis Date = 09/09/14 SpikeMix = Accu 214031115: 10 µl & NSI 032614: 10 µl Pct Recovery = 113% Analysis Date = 09/09/14 SpikeMix = NSI 032614: 10 µl & Spex Organics C1140417015: 10 µl Pct Recovery = 111% Analysis Date = 07/29/14 SpikeMix = Crescent 03DD004: 10 µl & NSI 032614: 10 µl Pct Recovery = 90% Analysis Date = 07/11/14 SpikeMix = Spex Organics C1140417015: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 109% Analysis Date = 05/30/14 SpikeMix = NSI 032614: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 85% Analysis Date = 03/17/16 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 92% Analysis Date = 01/27/16 SpikeMix = Crescent 04EE008: 10 µl & NSI 050515AVOC: 10 µl Pct Recovery = 88% Analysis Date = 12/10/15 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 90% Analysis Date = 09/03/15 SpikeMix = NSI 050515AVOC: 10 µl & Spex Organics EN150428007: 10 µl Pct Recovery = 82% Analysis Date = 11/20/15 SpikeMix = Accu 215041380: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 106% Analysis Date = 08/07/15 SpikeMix = Crescent 04EE008: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 105% Analysis Date = 06/27/15 SpikeMix = ERA 0406-15-03: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 109% Analysis Date = 12/15/16 Pct Recovery = 98% Analysis Date = 12/11/16 Pct Recovery = 98% Analysis Date = 12/11/16 Pct Recovery = 98% Analysis Date = 12/06/16 Pct Recovery = 98% Analysis Date = 12/06/16 Pct Recovery = 98% Analysis Date = 12/01/16 Pct Recovery = 98% Analysis Date = 12/01/16 Pct Recovery = 98% Analysis Date = 11/26/16 Pct Recovery = 98% Analysis Date = 11/26/16 Pct Recovery = 98% Analysis Date = 11/21/16 Pct Recovery = 98% Analysis Date = 11/21/16 Pct Recovery = 98% Analysis Date = 11/17/16 Pct Recovery = 98% Analysis Date = 11/17/16 Pct Recovery = 98% Analysis Date = 11/12/16 Pct Recovery = 98% Analysis Date = 11/12/16 Pct Recovery = 98% Analysis Date = 11/07/16 Pct Recovery = 98% Analysis Date = 11/07/16 Pct Recovery = 98% Analysis Date = 11/02/16 Pct Recovery = 98% Analysis Date = 11/02/16 Pct Recovery = 98% Analysis Date = 10/28/16 Pct Recovery = 98% Analysis Date = 10/28/16 Pct Recovery = 98% Analysis Date = 10/24/16 Pct Recovery = 98% Analysis Date = 10/24/16 Pct Recovery = 98% Analysis Date = 10/19/16 Pct Recovery = 98% Analysis Date = 10/19/16 Pct Recovery = 98% Analysis Date = 10/14/16 Pct Recovery = 98% Analysis Date = 10/14/16 Pct Recovery = 98% Analysis Date = 10/09/16 Pct Recovery = 98% Analysis Date = 10/09/16 Pct Recovery = 98% Analysis Date = 10/04/16 Pct Recovery = 98% Analysis Date = 10/04/16 Pct Recovery = 98% Analysis Date = 09/30/16 Pct Recovery = 98% Analysis Date = 09/30/16 Pct Recovery = 98% Analysis Date = 09/25/16 Pct Recovery = 98% Analysis Date = 09/25/16 Pct Recovery = 98% Analysis Date = 09/20/16 Pct Recovery = 98% Analysis Date = 09/20/16 Pct Recovery = 98% Analysis Date = 09/15/16 Pct Recovery = 98% Analysis Date = 09/15/16 Pct Recovery = 98% Analysis Date = 09/10/16 Pct Recovery = 98% Analysis Date = 09/10/16 Pct Recovery = 98% Analysis Date = 09/06/16 Pct Recovery = 98% Analysis Date = 09/06/16 Pct Recovery = 98% Analysis Date = 09/01/16 Pct Recovery = 98% Analysis Date = 09/01/16 Pct Recovery = 98% Analysis Date = 08/27/16 Pct Recovery = 97% Analysis Date = 08/27/16 Pct Recovery = 97% Analysis Date = 08/22/16 Pct Recovery = 97% Analysis Date = 08/22/16 Pct Recovery = 97% Analysis Date = 08/17/16 Pct Recovery = 97% Analysis Date = 08/17/16 Pct Recovery = 97% Analysis Date = 08/13/16 Pct Recovery = 97% Analysis Date = 08/13/16 Pct Recovery = 97% Analysis Date = 08/08/16 Pct Recovery = 97% Analysis Date = 08/08/16 Pct Recovery = 97% Analysis Date = 08/03/16 Pct Recovery = 97% Analysis Date = 08/03/16 Pct Recovery = 97% Analysis Date = 07/29/16 Pct Recovery = 97% Analysis Date = 07/29/16 Pct Recovery = 97% Analysis Date = 07/24/16 Pct Recovery = 97% Analysis Date = 07/24/16 Pct Recovery = 97% Analysis Date = 07/20/16 Pct Recovery = 97% Analysis Date = 07/20/16 Pct Recovery = 97% Analysis Date = 07/15/16 Pct Recovery = 97% Analysis Date = 07/15/16 Pct Recovery = 97% Analysis Date = 07/10/16 Pct Recovery = 97% Analysis Date = 07/10/16 Pct Recovery = 97% Analysis Date = 07/05/16 Pct Recovery = 97% Analysis Date = 07/05/16 Pct Recovery = 97% Analysis Date = 06/30/16 Pct Recovery = 97% Analysis Date = 06/30/16 Pct Recovery = 97% Analysis Date = 06/26/16 Pct Recovery = 97% Analysis Date = 06/26/16 Pct Recovery = 97% Analysis Date = 06/21/16 Pct Recovery = 97% Analysis Date = 06/21/16 Pct Recovery = 97% Analysis Date = 06/16/16 Pct Recovery = 97% Analysis Date = 06/16/16 Pct Recovery = 97% Analysis Date = 06/11/16 Pct Recovery = 97% Analysis Date = 06/11/16 Pct Recovery = 97% Analysis Date = 06/06/16 Pct Recovery = 97% Analysis Date = 06/06/16 Pct Recovery = 97% Analysis Date = 06/02/16 Pct Recovery = 97% Analysis Date = 06/02/16 Pct Recovery = 97% Analysis Date = 05/28/16 Pct Recovery = 97% Analysis Date = 05/28/16 Pct Recovery = 97% Analysis Date = 05/23/16 Pct Recovery = 97% Analysis Date = 05/23/16 Pct Recovery = 97% Analysis Date = 05/18/16 Pct Recovery = 97% Analysis Date = 05/18/16 Pct Recovery = 97% Analysis Date = 05/13/16 Pct Recovery = 97% Analysis Date = 05/13/16 Pct Recovery = 97% Analysis Date = 05/09/16 Pct Recovery = 97% Analysis Date = 05/09/16 Pct Recovery = 97% Analysis Date = 05/04/16 Pct Recovery = 97% Analysis Date = 05/04/16 Pct Recovery = 97% Analysis Date = 04/29/16 Pct Recovery = 97% Analysis Date = 04/29/16 Pct Recovery = 97% Analysis Date = 04/24/16 Pct Recovery = 97% Analysis Date = 04/24/16 Pct Recovery = 97% Analysis Date = 04/19/16 Pct Recovery = 97% Analysis Date = 04/19/16 Pct Recovery = 97% Analysis Date = 04/15/16 Pct Recovery = 97% Analysis Date = 04/15/16 Pct Recovery = 97% Analysis Date = 04/10/16 Pct Recovery = 97% Analysis Date = 04/10/16 Pct Recovery = 97% Analysis Date = 04/05/16 Pct Recovery = 97% Analysis Date = 04/05/16 Pct Recovery = 97% Analysis Date = 03/31/16 Pct Recovery = 97% Analysis Date = 03/31/16 Pct Recovery = 97% Analysis Date = 03/26/16 Pct Recovery = 97% Analysis Date = 03/26/16 Pct Recovery = 97% Analysis Date = 03/22/16 Pct Recovery = 97% Analysis Date = 03/22/16 Pct Recovery = 97% Analysis Date = 03/17/16 Pct Recovery = 97% Analysis Date = 03/17/16 Pct Recovery = 97% Analysis Date = 03/12/16 Pct Recovery = 97% Analysis Date = 03/12/16 Pct Recovery = 97% Analysis Date = 03/07/16 Pct Recovery = 97% Analysis Date = 03/07/16 Pct Recovery = 97% Analysis Date = 03/02/16 Pct Recovery = 97% Analysis Date = 03/02/16 Pct Recovery = 97% Analysis Date = 02/27/16 Pct Recovery = 97% Analysis Date = 02/27/16 Pct Recovery = 97% Analysis Date = 02/22/16 Pct Recovery = 97% Analysis Date = 02/22/16 Pct Recovery = 97% Analysis Date = 02/17/16 Pct Recovery = 97% Analysis Date = 02/17/16 Pct Recovery = 97% Analysis Date = 02/12/16 Pct Recovery = 97% Analysis Date = 02/12/16 Pct Recovery = 97% Analysis Date = 02/07/16 Pct Recovery = 97% Analysis Date = 02/07/16 Pct Recovery = 97% Analysis Date = 02/03/16 Pct Recovery = 97% Analysis Date = 02/03/16 Pct Recovery = 97% Analysis Date = 01/29/16 Pct Recovery = 97% Analysis Date = 01/29/16 Pct Recovery = 97% Analysis Date = 01/24/16 Pct Recovery = 97% Analysis Date = 01/24/16 Pct Recovery = 97% Analysis Date = 01/19/16 Pct Recovery = 97% Analysis Date = 01/19/16 Pct Recovery = 97% Analysis Date = 01/14/16 Pct Recovery = 97% Analysis Date = 01/14/16 Pct Recovery = 97% Analysis Date = 01/10/16 Pct Recovery = 97% Analysis Date = 01/10/16 Pct Recovery = 97% Analysis Date = 01/05/16 Pct Recovery = 97% Analysis Date = 01/05/16 Pct Recovery = 97% Analysis Date = 12/31/15 Pct Recovery = 97% Analysis Date = 12/31/15 Pct Recovery = 97% Analysis Date = 12/26/15 Pct Recovery = 97% Analysis Date = 12/26/15 Pct Recovery = 97% Analysis Date = 12/21/15 Pct Recovery = 97% Analysis Date = 12/21/15 Pct Recovery = 97% Analysis Date = 12/17/15 Pct Recovery = 97% Analysis Date = 12/17/15 Pct Recovery = 97% Analysis Date = 12/12/15 Pct Recovery = 96% Analysis Date = 12/12/15 Pct Recovery = 96% Analysis Date = 12/07/15 Pct Recovery = 96% Analysis Date = 12/07/15 Pct Recovery = 96% Analysis Date = 12/02/15 Pct Recovery = 96% Analysis Date = 12/02/15 Pct Recovery = 96% Analysis Date = 11/27/15 Pct Recovery = 96% Analysis Date = 11/27/15 Pct Recovery = 96% Analysis Date = 11/23/15 Pct Recovery = 96% Analysis Date = 11/23/15 Pct Recovery = 96% Analysis Date = 11/18/15 Pct Recovery = 96% Analysis Date = 11/18/15 Pct Recovery = 96% Analysis Date = 11/13/15 Pct Recovery = 96% Analysis Date = 11/13/15 Pct Recovery = 96% Analysis Date = 11/08/15 Pct Recovery = 96% Analysis Date = 11/08/15 Pct Recovery = 96% Analysis Date = 11/03/15 Pct Recovery = 96% Analysis Date = 11/03/15 Pct Recovery = 96% Analysis Date = 10/30/15 Pct Recovery = 96% Analysis Date = 10/30/15 Pct Recovery = 96% Analysis Date = 10/25/15 Pct Recovery = 96% Analysis Date = 10/25/15 Pct Recovery = 96% Analysis Date = 10/20/15 Pct Recovery = 96% Analysis Date = 10/20/15 Pct Recovery = 96% Analysis Date = 10/15/15 Pct Recovery = 96% Analysis Date = 10/15/15 Pct Recovery = 96% Analysis Date = 10/10/15 Pct Recovery = 96% Analysis Date = 10/10/15 Pct Recovery = 96% Analysis Date = 10/06/15 Pct Recovery = 96% Analysis Date = 10/06/15 Pct Recovery = 96% Analysis Date = 10/01/15 Pct Recovery = 96% Analysis Date = 10/01/15 Pct Recovery = 96% Analysis Date = 09/26/15 Pct Recovery = 96% Analysis Date = 09/26/15 Pct Recovery = 96% Analysis Date = 09/21/15 Pct Recovery = 96% Analysis Date = 09/21/15 Pct Recovery = 96% Analysis Date = 09/16/15 Pct Recovery = 96% Analysis Date = 09/16/15 Pct Recovery = 96% Analysis Date = 09/12/15 Pct Recovery = 96% Analysis Date = 09/12/15 Pct Recovery = 96% Analysis Date = 09/07/15 Pct Recovery = 96% Analysis Date = 09/07/15 Pct Recovery = 96% Analysis Date = 09/02/15 Pct Recovery = 96% Analysis Date = 09/02/15 Pct Recovery = 96% Analysis Date = 08/28/15 Pct Recovery = 96% Analysis Date = 08/28/15 Pct Recovery = 96% Analysis Date = 08/23/15 Pct Recovery = 96% Analysis Date = 08/23/15 Pct Recovery = 96% Analysis Date = 08/19/15 Pct Recovery = 96% Analysis Date = 08/19/15 Pct Recovery = 96% Analysis Date = 08/14/15 Pct Recovery = 96% Analysis Date = 08/14/15 Pct Recovery = 96% Analysis Date = 08/09/15 Pct Recovery = 96% Analysis Date = 08/09/15 Pct Recovery = 96% Analysis Date = 08/04/15 Pct Recovery = 96% Analysis Date = 08/04/15 Pct Recovery = 96% Analysis Date = 07/30/15 Pct Recovery = 96% Analysis Date = 07/30/15 Pct Recovery = 96% Analysis Date = 07/26/15 Pct Recovery = 96% Analysis Date = 07/26/15 Pct Recovery = 96% Analysis Date = 07/21/15 Pct Recovery = 96% Analysis Date = 07/21/15 Pct Recovery = 96% Analysis Date = 07/16/15 Pct Recovery = 96% Analysis Date = 07/16/15 Pct Recovery = 96% Analysis Date = 07/11/15 Pct Recovery = 96% Analysis Date = 07/11/15 Pct Recovery = 96% Analysis Date = 07/06/15 Pct Recovery = 96% Analysis Date = 07/06/15 Pct Recovery = 96% Analysis Date = 07/02/15 Pct Recovery = 97% Analysis Date = 07/02/15 Pct Recovery = 97% Analysis Date = 06/27/15 Pct Recovery = 97% Analysis Date = 06/27/15 Pct Recovery = 97% Analysis Date = 06/22/15 Pct Recovery = 97% Analysis Date = 06/22/15 Pct Recovery = 97% Analysis Date = 06/17/15 Pct Recovery = 97% Analysis Date = 06/17/15 Pct Recovery = 97% Analysis Date = 06/12/15 Pct Recovery = 97% Analysis Date = 06/12/15 Pct Recovery = 97% Analysis Date = 06/08/15 Pct Recovery = 97% Analysis Date = 06/08/15 Pct Recovery = 97% Analysis Date = 06/03/15 Pct Recovery = 97% Analysis Date = 06/03/15 Pct Recovery = 97% Analysis Date = 05/29/15 Pct Recovery = 97% Analysis Date = 05/29/15 Pct Recovery = 97% Analysis Date = 05/24/15 Pct Recovery = 97% Analysis Date = 05/24/15 Pct Recovery = 97% Analysis Date = 05/19/15 Pct Recovery = 97% Analysis Date = 05/19/15 Pct Recovery = 97% Analysis Date = 05/15/15 Pct Recovery = 97% Analysis Date = 05/15/15 Pct Recovery = 97% Analysis Date = 05/10/15 Pct Recovery = 97% Analysis Date = 05/10/15 Pct Recovery = 97% Analysis Date = 05/05/15 Pct Recovery = 97% Analysis Date = 05/05/15 Pct Recovery = 97% Analysis Date = 04/30/15 Pct Recovery = 97% Analysis Date = 04/30/15 Pct Recovery = 97% Analysis Date = 04/25/15 Pct Recovery = 97% Analysis Date = 04/25/15 Pct Recovery = 97% Analysis Date = 04/21/15 Pct Recovery = 97% Analysis Date = 04/21/15 Pct Recovery = 97% Analysis Date = 04/16/15 Pct Recovery = 97% Analysis Date = 04/16/15 Pct Recovery = 97% Analysis Date = 04/11/15 Pct Recovery = 97% Analysis Date = 04/11/15 Pct Recovery = 97% Analysis Date = 04/06/15 Pct Recovery = 98% Analysis Date = 04/06/15 Pct Recovery = 98% Analysis Date = 04/01/15 Pct Recovery = 98% Analysis Date = 04/01/15 Pct Recovery = 98% Analysis Date = 03/28/15 Pct Recovery = 98% Analysis Date = 03/28/15 Pct Recovery = 98% Analysis Date = 03/23/15 Pct Recovery = 98% Analysis Date = 03/23/15 Pct Recovery = 98% Analysis Date = 03/18/15 Pct Recovery = 98% Analysis Date = 03/18/15 Pct Recovery = 98% Analysis Date = 03/13/15 Pct Recovery = 98% Analysis Date = 03/13/15 Pct Recovery = 98% Analysis Date = 03/08/15 Pct Recovery = 98% Analysis Date = 03/08/15 Pct Recovery = 98% Analysis Date = 03/04/15 Pct Recovery = 98% Analysis Date = 03/04/15 Pct Recovery = 98% Analysis Date = 02/27/15 Pct Recovery = 98% Analysis Date = 02/27/15 Pct Recovery = 98% Analysis Date = 02/22/15 Pct Recovery = 98% Analysis Date = 02/22/15 Pct Recovery = 98% Analysis Date = 02/17/15 Pct Recovery = 98% Analysis Date = 02/17/15 Pct Recovery = 98% Analysis Date = 02/12/15 Pct Recovery = 98% Analysis Date = 02/12/15 Pct Recovery = 98% Analysis Date = 02/08/15 Pct Recovery = 98% Analysis Date = 02/08/15 Pct Recovery = 98% Analysis Date = 02/03/15 Pct Recovery = 98% Analysis Date = 02/03/15 Pct Recovery = 98% Analysis Date = 01/29/15 Pct Recovery = 98% Analysis Date = 01/29/15 Pct Recovery = 98% Analysis Date = 01/24/15 Pct Recovery = 98% Analysis Date = 01/24/15 Pct Recovery = 98% Analysis Date = 01/19/15 Pct Recovery = 98% Analysis Date = 01/19/15 Pct Recovery = 98% Analysis Date = 01/15/15 Pct Recovery = 98% Analysis Date = 01/15/15 Pct Recovery = 98% Analysis Date = 01/10/15 Pct Recovery = 98% Analysis Date = 01/10/15 Pct Recovery = 98% Analysis Date = 01/05/15 Pct Recovery = 98% Analysis Date = 01/05/15 Pct Recovery = 98% Analysis Date = 12/31/14 Pct Recovery = 98% Analysis Date = 12/31/14 Pct Recovery = 98% Analysis Date = 12/26/14 Pct Recovery = 98% Analysis Date = 12/26/14 Pct Recovery = 98% Analysis Date = 12/22/14 Pct Recovery = 98% Analysis Date = 12/22/14 Pct Recovery = 98% Analysis Date = 12/17/14 Pct Recovery = 98% Analysis Date = 12/17/14 Pct Recovery = 98% Analysis Date = 12/12/14 Pct Recovery = 98% Analysis Date = 12/12/14 Pct Recovery = 98% Analysis Date = 12/07/14 Pct Recovery = 98% Analysis Date = 12/07/14 Pct Recovery = 98% Analysis Date = 12/02/14 Pct Recovery = 98% Analysis Date = 12/02/14 Pct Recovery = 98% Analysis Date = 11/28/14 Pct Recovery = 98% Analysis Date = 11/28/14 Pct Recovery = 98% Analysis Date = 11/23/14 Pct Recovery = 98% Analysis Date = 11/23/14 Pct Recovery = 98% Analysis Date = 11/18/14 Pct Recovery = 98% Analysis Date = 11/18/14 Pct Recovery = 98% Analysis Date = 11/13/14 Pct Recovery = 98% Analysis Date = 11/13/14 Pct Recovery = 98% Analysis Date = 11/08/14 Pct Recovery = 99% Analysis Date = 11/08/14 Pct Recovery = 99% Analysis Date = 11/04/14 Pct Recovery = 99% Analysis Date = 11/04/14 Pct Recovery = 99% Analysis Date = 10/30/14 Pct Recovery = 99% Analysis Date = 10/30/14 Pct Recovery = 99% Analysis Date = 10/25/14 Pct Recovery = 99% Analysis Date = 10/25/14 Pct Recovery = 99% Analysis Date = 10/20/14 Pct Recovery = 99% Analysis Date = 10/20/14 Pct Recovery = 99% Analysis Date = 10/15/14 Pct Recovery = 99% Analysis Date = 10/15/14 Pct Recovery = 99% Analysis Date = 10/11/14 Pct Recovery = 99% Analysis Date = 10/11/14 Pct Recovery = 99% Analysis Date = 10/06/14 Pct Recovery = 99% Analysis Date = 10/06/14 Pct Recovery = 99% Analysis Date = 10/01/14 Pct Recovery = 99% Analysis Date = 10/01/14 Pct Recovery = 99% Analysis Date = 09/26/14 Pct Recovery = 99% Analysis Date = 09/26/14 Pct Recovery = 99% Analysis Date = 09/21/14 Pct Recovery = 99% Analysis Date = 09/21/14 Pct Recovery = 99% Analysis Date = 09/17/14 Pct Recovery = 99% Analysis Date = 09/17/14 Pct Recovery = 99% Analysis Date = 09/12/14 Pct Recovery = 99% Analysis Date = 09/12/14 Pct Recovery = 99% Analysis Date = 09/07/14 Pct Recovery = 99% Analysis Date = 09/07/14 Pct Recovery = 99% Analysis Date = 09/02/14 Pct Recovery = 99% Analysis Date = 09/02/14 Pct Recovery = 99% Analysis Date = 08/28/14 Pct Recovery = 99% Analysis Date = 08/28/14 Pct Recovery = 99% Analysis Date = 08/24/14 Pct Recovery = 99% Analysis Date = 08/24/14 Pct Recovery = 99% Analysis Date = 08/19/14 Pct Recovery = 99% Analysis Date = 08/19/14 Pct Recovery = 99% Analysis Date = 08/14/14 Pct Recovery = 99% Analysis Date = 08/14/14 Pct Recovery = 99% Analysis Date = 08/09/14 Pct Recovery = 99% Analysis Date = 08/09/14 Pct Recovery = 99% Analysis Date = 08/04/14 Pct Recovery = 99% Analysis Date = 08/04/14 Pct Recovery = 99% Analysis Date = 07/31/14 Pct Recovery = 99% Analysis Date = 07/31/14 Pct Recovery = 99% Analysis Date = 07/26/14 Pct Recovery = 99% Analysis Date = 07/26/14 Pct Recovery = 99% Analysis Date = 07/21/14 Pct Recovery = 99% Analysis Date = 07/21/14 Pct Recovery = 99% Analysis Date = 07/16/14 Pct Recovery = 99% Analysis Date = 07/16/14 Pct Recovery = 99% Analysis Date = 07/11/14 Pct Recovery = 99% Analysis Date = 07/11/14 Pct Recovery = 99% Analysis Date = 07/07/14 Pct Recovery = 98% Analysis Date = 07/07/14 Pct Recovery = 98% Analysis Date = 07/02/14 Pct Recovery = 98% Analysis Date = 07/02/14 Pct Recovery = 98% Analysis Date = 06/27/14 Pct Recovery = 98% Analysis Date = 06/27/14 Pct Recovery = 98% Analysis Date = 06/22/14 Pct Recovery = 98% Analysis Date = 06/22/14 Pct Recovery = 98% Analysis Date = 06/17/14 Pct Recovery = 98% Analysis Date = 06/17/14 Pct Recovery = 98% Analysis Date = 06/13/14 Pct Recovery = 98% Analysis Date = 06/13/14 Pct Recovery = 98% Analysis Date = 06/08/14 Pct Recovery = 98% Analysis Date = 06/08/14 Pct Recovery = 98% Analysis Date = 06/03/14 Pct Recovery = 98% Analysis Date = 06/03/14 Pct Recovery = 98% Analysis Date = 05/29/14 Pct Recovery = 98% Analysis Date = 05/29/14 Pct Recovery = 98% Analysis Date = 05/24/14 Pct Recovery = 98% Analysis Date = 05/24/14 Pct Recovery = 98% Analysis Date = 05/20/14 Pct Recovery = 98% Analysis Date = 05/20/14 Pct Recovery = 98% Analysis Date = 05/15/14 Pct Recovery = 98% Analysis Date = 05/15/14 Pct Recovery = 98% Analysis Date = 05/10/14 Pct Recovery = 98% Analysis Date = 05/10/14 Pct Recovery = 98% Analysis Date = 05/05/14 Pct Recovery = 98% Analysis Date = 05/05/14 Pct Recovery = 98% Analysis Date = 05/01/14 Pct Recovery = 98% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
TERT-PENTYL METHYL ETHER (TAME)

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 48 97% 10% 97% 11%
Total 48 97% 10% 97% 11%

Sample Statistics
TERT-PENTYL METHYL ETHER (TAME)

Characteristic N % % Basis
Plotted 48 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 48 .  
False Negatives 0 0% 0 out of 48
Not Spiked 25 .  
False Positives 0 0% 0 out of 25

BQS OBSP Determination:
TETRACHLOROETHYLENE
METHOD: 4440 , TESTIDCODE: 34475GCM66
Open Data Set

Analysis Date = 12/12/16 SpikeMix = Accu 216041125: 40 µl & Crescent 03FF058: 40 µl Pct Recovery = 101% Analysis Date = 07/20/16 SpikeMix = Supelco LC20141V: 40 µl & Accu 216041125: 40 µl Pct Recovery = 94% Analysis Date = 07/14/16 SpikeMix = Accu 216041125: 40 µl & NSI 041816AVOC: 40 µl Pct Recovery = 113% Analysis Date = 09/08/16 SpikeMix = Supelco LC20141V: 25 µl & Accu 216041125: 25 µl Pct Recovery = 127% Analysis Date = 05/24/16 SpikeMix = Accu 216041125: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 90% Analysis Date = 08/12/16 SpikeMix = ChemService 5082900: 25 µl & Phenova B20160319: 25 µl Pct Recovery = 127% Analysis Date = 06/21/16 SpikeMix = Phenova B20160319: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 136% Analysis Date = 03/19/15 SpikeMix = Spex Organics C1140417015: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 123% Analysis Date = 03/06/15 SpikeMix = ERA 0227-14-06.1A: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 99% Analysis Date = 12/17/14 SpikeMix = Supelco LC06438: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 94% Analysis Date = 11/22/14 SpikeMix = NSI 032614: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 131% Analysis Date = 09/21/14 SpikeMix = Supelco LC06438: 20 µl Pct Recovery = 105% Analysis Date = 08/19/14 SpikeMix = Spex Organics C1140417015: 20 µl & Accu 214031115: 20 µl Pct Recovery = 124% Analysis Date = 08/16/14 SpikeMix = ERA 0227-14-06.1A: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 114% Analysis Date = 06/10/14 SpikeMix = NSI 032614: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 113% Analysis Date = 09/29/15 SpikeMix = Accu 215041380: 25 µl & ERA 0406-15-03: 25 µl Pct Recovery = 101% Analysis Date = 06/16/15 SpikeMix = ERA 0406-15-03: 25 µl & Supelco LC13545: 25 µl Pct Recovery = 90% Analysis Date = 07/13/15 SpikeMix = Crescent 04EE008: 25 µl & NSI 050515AVOC: 25 µl Pct Recovery = 99% Analysis Date = 10/13/16 SpikeMix = Accu 216041125: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 127% Analysis Date = 08/20/16 SpikeMix = Accu 216041125: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 159% Analysis Date = 06/30/16 SpikeMix = ChemService 5082900: 15 µl & Accu 216041125: 15 µl Pct Recovery = 125% Analysis Date = 11/29/16 SpikeMix = ChemService 5082900: 15 µl & Phenova B20160319: 15 µl Pct Recovery = 92% Analysis Date = 09/08/16 SpikeMix = Phenova B20160319: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 128% Analysis Date = 07/29/16 SpikeMix = Phenova B20160319: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 125% Analysis Date = 05/27/16 SpikeMix = Phenova B20160319: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 97% Analysis Date = 04/26/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 112% Analysis Date = 03/04/16 SpikeMix = Accu 215041380: 15 µl & ERA 0406-15-03: 15 µl Pct Recovery = 91% Analysis Date = 02/05/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 98% Analysis Date = 10/16/15 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 114% Analysis Date = 11/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 97% Analysis Date = 10/17/15 SpikeMix = Crescent 04EE008: 15 µl & NSI 050515AVOC: 15 µl Pct Recovery = 98% Analysis Date = 06/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Accu 215041380: 15 µl Pct Recovery = 104% Analysis Date = 11/06/14 SpikeMix = Spex Organics C1140417015: 10 µl & Crescent 03DD004: 10 µl Pct Recovery = 117% Analysis Date = 10/21/14 SpikeMix = ERA 0227-14-06.1A: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 114% Analysis Date = 09/09/14 SpikeMix = NSI 032614: 10 µl & Spex Organics C1140417015: 10 µl Pct Recovery = 125% Analysis Date = 07/23/14 SpikeMix = Spex Organics C1140417015: 10 µl & Accu 214031115: 10 µl Pct Recovery = 135% Analysis Date = 07/11/14 SpikeMix = Spex Organics C1140417015: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 114% Analysis Date = 06/18/14 SpikeMix = Supelco LC06438: 10 µl & Accu 214031115: 10 µl Pct Recovery = 124% Analysis Date = 05/30/14 SpikeMix = NSI 032614: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 110% Analysis Date = 05/03/14 SpikeMix = Crescent 03DD004: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 113% Analysis Date = 11/20/15 SpikeMix = Accu 215041380: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 94% Analysis Date = 07/31/15 SpikeMix = Crescent 04EE008: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 88% Analysis Date = 06/27/15 SpikeMix = ERA 0406-15-03: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 110% Analysis Date = 03/17/16 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 157% Analysis Date = 01/27/16 SpikeMix = Crescent 04EE008: 10 µl & NSI 050515AVOC: 10 µl Pct Recovery = 100% Analysis Date = 12/10/15 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 111% Analysis Date = 09/03/15 SpikeMix = NSI 050515AVOC: 10 µl & Spex Organics EN150428007: 10 µl Pct Recovery = 127% Analysis Date = 12/12/16 Pct Recovery = 120% Analysis Date = 12/07/16 Pct Recovery = 120% Analysis Date = 12/07/16 Pct Recovery = 120% Analysis Date = 12/02/16 Pct Recovery = 120% Analysis Date = 12/02/16 Pct Recovery = 120% Analysis Date = 11/27/16 Pct Recovery = 120% Analysis Date = 11/27/16 Pct Recovery = 120% Analysis Date = 11/22/16 Pct Recovery = 120% Analysis Date = 11/22/16 Pct Recovery = 120% Analysis Date = 11/18/16 Pct Recovery = 120% Analysis Date = 11/18/16 Pct Recovery = 120% Analysis Date = 11/13/16 Pct Recovery = 120% Analysis Date = 11/13/16 Pct Recovery = 120% Analysis Date = 11/08/16 Pct Recovery = 119% Analysis Date = 11/08/16 Pct Recovery = 119% Analysis Date = 11/03/16 Pct Recovery = 119% Analysis Date = 11/03/16 Pct Recovery = 119% Analysis Date = 10/30/16 Pct Recovery = 119% Analysis Date = 10/30/16 Pct Recovery = 119% Analysis Date = 10/25/16 Pct Recovery = 119% Analysis Date = 10/25/16 Pct Recovery = 119% Analysis Date = 10/20/16 Pct Recovery = 119% Analysis Date = 10/20/16 Pct Recovery = 119% Analysis Date = 10/15/16 Pct Recovery = 119% Analysis Date = 10/15/16 Pct Recovery = 119% Analysis Date = 10/10/16 Pct Recovery = 119% Analysis Date = 10/10/16 Pct Recovery = 119% Analysis Date = 10/06/16 Pct Recovery = 119% Analysis Date = 10/06/16 Pct Recovery = 119% Analysis Date = 10/01/16 Pct Recovery = 119% Analysis Date = 10/01/16 Pct Recovery = 119% Analysis Date = 09/26/16 Pct Recovery = 118% Analysis Date = 09/26/16 Pct Recovery = 118% Analysis Date = 09/21/16 Pct Recovery = 118% Analysis Date = 09/21/16 Pct Recovery = 118% Analysis Date = 09/17/16 Pct Recovery = 118% Analysis Date = 09/17/16 Pct Recovery = 118% Analysis Date = 09/12/16 Pct Recovery = 118% Analysis Date = 09/12/16 Pct Recovery = 118% Analysis Date = 09/07/16 Pct Recovery = 118% Analysis Date = 09/07/16 Pct Recovery = 118% Analysis Date = 09/02/16 Pct Recovery = 118% Analysis Date = 09/02/16 Pct Recovery = 118% Analysis Date = 08/29/16 Pct Recovery = 118% Analysis Date = 08/29/16 Pct Recovery = 118% Analysis Date = 08/24/16 Pct Recovery = 118% Analysis Date = 08/24/16 Pct Recovery = 118% Analysis Date = 08/19/16 Pct Recovery = 118% Analysis Date = 08/19/16 Pct Recovery = 118% Analysis Date = 08/14/16 Pct Recovery = 117% Analysis Date = 08/14/16 Pct Recovery = 117% Analysis Date = 08/09/16 Pct Recovery = 117% Analysis Date = 08/09/16 Pct Recovery = 117% Analysis Date = 08/05/16 Pct Recovery = 117% Analysis Date = 08/05/16 Pct Recovery = 117% Analysis Date = 07/31/16 Pct Recovery = 117% Analysis Date = 07/31/16 Pct Recovery = 117% Analysis Date = 07/26/16 Pct Recovery = 117% Analysis Date = 07/26/16 Pct Recovery = 117% Analysis Date = 07/21/16 Pct Recovery = 117% Analysis Date = 07/21/16 Pct Recovery = 117% Analysis Date = 07/17/16 Pct Recovery = 117% Analysis Date = 07/17/16 Pct Recovery = 117% Analysis Date = 07/12/16 Pct Recovery = 117% Analysis Date = 07/12/16 Pct Recovery = 117% Analysis Date = 07/07/16 Pct Recovery = 116% Analysis Date = 07/07/16 Pct Recovery = 116% Analysis Date = 07/02/16 Pct Recovery = 116% Analysis Date = 07/02/16 Pct Recovery = 116% Analysis Date = 06/28/16 Pct Recovery = 116% Analysis Date = 06/28/16 Pct Recovery = 116% Analysis Date = 06/23/16 Pct Recovery = 116% Analysis Date = 06/23/16 Pct Recovery = 116% Analysis Date = 06/18/16 Pct Recovery = 116% Analysis Date = 06/18/16 Pct Recovery = 116% Analysis Date = 06/13/16 Pct Recovery = 116% Analysis Date = 06/13/16 Pct Recovery = 116% Analysis Date = 06/08/16 Pct Recovery = 116% Analysis Date = 06/08/16 Pct Recovery = 116% Analysis Date = 06/04/16 Pct Recovery = 115% Analysis Date = 06/04/16 Pct Recovery = 115% Analysis Date = 05/30/16 Pct Recovery = 115% Analysis Date = 05/30/16 Pct Recovery = 115% Analysis Date = 05/25/16 Pct Recovery = 115% Analysis Date = 05/25/16 Pct Recovery = 115% Analysis Date = 05/20/16 Pct Recovery = 115% Analysis Date = 05/20/16 Pct Recovery = 115% Analysis Date = 05/16/16 Pct Recovery = 115% Analysis Date = 05/16/16 Pct Recovery = 115% Analysis Date = 05/11/16 Pct Recovery = 114% Analysis Date = 05/11/16 Pct Recovery = 114% Analysis Date = 05/06/16 Pct Recovery = 114% Analysis Date = 05/06/16 Pct Recovery = 114% Analysis Date = 05/01/16 Pct Recovery = 114% Analysis Date = 05/01/16 Pct Recovery = 114% Analysis Date = 04/27/16 Pct Recovery = 114% Analysis Date = 04/27/16 Pct Recovery = 114% Analysis Date = 04/22/16 Pct Recovery = 114% Analysis Date = 04/22/16 Pct Recovery = 114% Analysis Date = 04/17/16 Pct Recovery = 113% Analysis Date = 04/17/16 Pct Recovery = 113% Analysis Date = 04/12/16 Pct Recovery = 113% Analysis Date = 04/12/16 Pct Recovery = 113% Analysis Date = 04/07/16 Pct Recovery = 113% Analysis Date = 04/07/16 Pct Recovery = 113% Analysis Date = 04/03/16 Pct Recovery = 112% Analysis Date = 04/03/16 Pct Recovery = 112% Analysis Date = 03/29/16 Pct Recovery = 112% Analysis Date = 03/29/16 Pct Recovery = 112% Analysis Date = 03/24/16 Pct Recovery = 112% Analysis Date = 03/24/16 Pct Recovery = 112% Analysis Date = 03/19/16 Pct Recovery = 111% Analysis Date = 03/19/16 Pct Recovery = 111% Analysis Date = 03/15/16 Pct Recovery = 111% Analysis Date = 03/15/16 Pct Recovery = 111% Analysis Date = 03/10/16 Pct Recovery = 111% Analysis Date = 03/10/16 Pct Recovery = 111% Analysis Date = 03/05/16 Pct Recovery = 110% Analysis Date = 03/05/16 Pct Recovery = 110% Analysis Date = 02/29/16 Pct Recovery = 110% Analysis Date = 02/29/16 Pct Recovery = 110% Analysis Date = 02/25/16 Pct Recovery = 110% Analysis Date = 02/25/16 Pct Recovery = 110% Analysis Date = 02/20/16 Pct Recovery = 109% Analysis Date = 02/20/16 Pct Recovery = 109% Analysis Date = 02/15/16 Pct Recovery = 109% Analysis Date = 02/15/16 Pct Recovery = 109% Analysis Date = 02/10/16 Pct Recovery = 109% Analysis Date = 02/10/16 Pct Recovery = 109% Analysis Date = 02/05/16 Pct Recovery = 108% Analysis Date = 02/05/16 Pct Recovery = 108% Analysis Date = 02/01/16 Pct Recovery = 108% Analysis Date = 02/01/16 Pct Recovery = 108% Analysis Date = 01/27/16 Pct Recovery = 108% Analysis Date = 01/27/16 Pct Recovery = 108% Analysis Date = 01/22/16 Pct Recovery = 108% Analysis Date = 01/22/16 Pct Recovery = 108% Analysis Date = 01/17/16 Pct Recovery = 108% Analysis Date = 01/17/16 Pct Recovery = 108% Analysis Date = 01/13/16 Pct Recovery = 107% Analysis Date = 01/13/16 Pct Recovery = 107% Analysis Date = 01/08/16 Pct Recovery = 107% Analysis Date = 01/08/16 Pct Recovery = 107% Analysis Date = 01/03/16 Pct Recovery = 107% Analysis Date = 01/03/16 Pct Recovery = 107% Analysis Date = 12/29/15 Pct Recovery = 107% Analysis Date = 12/29/15 Pct Recovery = 107% Analysis Date = 12/25/15 Pct Recovery = 107% Analysis Date = 12/25/15 Pct Recovery = 107% Analysis Date = 12/20/15 Pct Recovery = 107% Analysis Date = 12/20/15 Pct Recovery = 107% Analysis Date = 12/15/15 Pct Recovery = 106% Analysis Date = 12/15/15 Pct Recovery = 106% Analysis Date = 12/10/15 Pct Recovery = 106% Analysis Date = 12/10/15 Pct Recovery = 106% Analysis Date = 12/05/15 Pct Recovery = 106% Analysis Date = 12/05/15 Pct Recovery = 106% Analysis Date = 12/01/15 Pct Recovery = 106% Analysis Date = 12/01/15 Pct Recovery = 106% Analysis Date = 11/26/15 Pct Recovery = 106% Analysis Date = 11/26/15 Pct Recovery = 106% Analysis Date = 11/21/15 Pct Recovery = 105% Analysis Date = 11/21/15 Pct Recovery = 105% Analysis Date = 11/16/15 Pct Recovery = 105% Analysis Date = 11/16/15 Pct Recovery = 105% Analysis Date = 11/12/15 Pct Recovery = 105% Analysis Date = 11/12/15 Pct Recovery = 105% Analysis Date = 11/07/15 Pct Recovery = 105% Analysis Date = 11/07/15 Pct Recovery = 105% Analysis Date = 11/02/15 Pct Recovery = 105% Analysis Date = 11/02/15 Pct Recovery = 105% Analysis Date = 10/28/15 Pct Recovery = 105% Analysis Date = 10/28/15 Pct Recovery = 105% Analysis Date = 10/24/15 Pct Recovery = 105% Analysis Date = 10/24/15 Pct Recovery = 105% Analysis Date = 10/19/15 Pct Recovery = 105% Analysis Date = 10/19/15 Pct Recovery = 105% Analysis Date = 10/14/15 Pct Recovery = 105% Analysis Date = 10/14/15 Pct Recovery = 105% Analysis Date = 10/09/15 Pct Recovery = 105% Analysis Date = 10/09/15 Pct Recovery = 105% Analysis Date = 10/04/15 Pct Recovery = 105% Analysis Date = 10/04/15 Pct Recovery = 105% Analysis Date = 09/30/15 Pct Recovery = 105% Analysis Date = 09/30/15 Pct Recovery = 105% Analysis Date = 09/25/15 Pct Recovery = 105% Analysis Date = 09/25/15 Pct Recovery = 105% Analysis Date = 09/20/15 Pct Recovery = 104% Analysis Date = 09/20/15 Pct Recovery = 104% Analysis Date = 09/15/15 Pct Recovery = 104% Analysis Date = 09/15/15 Pct Recovery = 104% Analysis Date = 09/11/15 Pct Recovery = 104% Analysis Date = 09/11/15 Pct Recovery = 104% Analysis Date = 09/06/15 Pct Recovery = 104% Analysis Date = 09/06/15 Pct Recovery = 104% Analysis Date = 09/01/15 Pct Recovery = 104% Analysis Date = 09/01/15 Pct Recovery = 104% Analysis Date = 08/27/15 Pct Recovery = 104% Analysis Date = 08/27/15 Pct Recovery = 104% Analysis Date = 08/23/15 Pct Recovery = 104% Analysis Date = 08/23/15 Pct Recovery = 104% Analysis Date = 08/18/15 Pct Recovery = 104% Analysis Date = 08/18/15 Pct Recovery = 104% Analysis Date = 08/13/15 Pct Recovery = 104% Analysis Date = 08/13/15 Pct Recovery = 104% Analysis Date = 08/08/15 Pct Recovery = 104% Analysis Date = 08/08/15 Pct Recovery = 104% Analysis Date = 08/03/15 Pct Recovery = 104% Analysis Date = 08/03/15 Pct Recovery = 104% Analysis Date = 07/30/15 Pct Recovery = 104% Analysis Date = 07/30/15 Pct Recovery = 104% Analysis Date = 07/25/15 Pct Recovery = 104% Analysis Date = 07/25/15 Pct Recovery = 104% Analysis Date = 07/20/15 Pct Recovery = 105% Analysis Date = 07/20/15 Pct Recovery = 105% Analysis Date = 07/15/15 Pct Recovery = 105% Analysis Date = 07/15/15 Pct Recovery = 105% Analysis Date = 07/11/15 Pct Recovery = 105% Analysis Date = 07/11/15 Pct Recovery = 105% Analysis Date = 07/06/15 Pct Recovery = 105% Analysis Date = 07/06/15 Pct Recovery = 105% Analysis Date = 07/01/15 Pct Recovery = 105% Analysis Date = 07/01/15 Pct Recovery = 105% Analysis Date = 06/26/15 Pct Recovery = 105% Analysis Date = 06/26/15 Pct Recovery = 105% Analysis Date = 06/21/15 Pct Recovery = 105% Analysis Date = 06/21/15 Pct Recovery = 105% Analysis Date = 06/17/15 Pct Recovery = 105% Analysis Date = 06/17/15 Pct Recovery = 105% Analysis Date = 06/12/15 Pct Recovery = 105% Analysis Date = 06/12/15 Pct Recovery = 105% Analysis Date = 06/07/15 Pct Recovery = 106% Analysis Date = 06/07/15 Pct Recovery = 106% Analysis Date = 06/02/15 Pct Recovery = 106% Analysis Date = 06/02/15 Pct Recovery = 106% Analysis Date = 05/29/15 Pct Recovery = 106% Analysis Date = 05/29/15 Pct Recovery = 106% Analysis Date = 05/24/15 Pct Recovery = 106% Analysis Date = 05/24/15 Pct Recovery = 106% Analysis Date = 05/19/15 Pct Recovery = 106% Analysis Date = 05/19/15 Pct Recovery = 106% Analysis Date = 05/14/15 Pct Recovery = 106% Analysis Date = 05/14/15 Pct Recovery = 106% Analysis Date = 05/10/15 Pct Recovery = 107% Analysis Date = 05/10/15 Pct Recovery = 107% Analysis Date = 05/05/15 Pct Recovery = 107% Analysis Date = 05/05/15 Pct Recovery = 107% Analysis Date = 04/30/15 Pct Recovery = 107% Analysis Date = 04/30/15 Pct Recovery = 107% Analysis Date = 04/25/15 Pct Recovery = 107% Analysis Date = 04/25/15 Pct Recovery = 107% Analysis Date = 04/20/15 Pct Recovery = 107% Analysis Date = 04/20/15 Pct Recovery = 107% Analysis Date = 04/16/15 Pct Recovery = 107% Analysis Date = 04/16/15 Pct Recovery = 107% Analysis Date = 04/11/15 Pct Recovery = 108% Analysis Date = 04/11/15 Pct Recovery = 108% Analysis Date = 04/06/15 Pct Recovery = 108% Analysis Date = 04/06/15 Pct Recovery = 108% Analysis Date = 04/01/15 Pct Recovery = 108% Analysis Date = 04/01/15 Pct Recovery = 108% Analysis Date = 03/28/15 Pct Recovery = 108% Analysis Date = 03/28/15 Pct Recovery = 108% Analysis Date = 03/23/15 Pct Recovery = 108% Analysis Date = 03/23/15 Pct Recovery = 108% Analysis Date = 03/18/15 Pct Recovery = 108% Analysis Date = 03/18/15 Pct Recovery = 108% Analysis Date = 03/13/15 Pct Recovery = 109% Analysis Date = 03/13/15 Pct Recovery = 109% Analysis Date = 03/09/15 Pct Recovery = 109% Analysis Date = 03/09/15 Pct Recovery = 109% Analysis Date = 03/04/15 Pct Recovery = 109% Analysis Date = 03/04/15 Pct Recovery = 109% Analysis Date = 02/27/15 Pct Recovery = 109% Analysis Date = 02/27/15 Pct Recovery = 109% Analysis Date = 02/22/15 Pct Recovery = 109% Analysis Date = 02/22/15 Pct Recovery = 109% Analysis Date = 02/17/15 Pct Recovery = 109% Analysis Date = 02/17/15 Pct Recovery = 109% Analysis Date = 02/13/15 Pct Recovery = 110% Analysis Date = 02/13/15 Pct Recovery = 110% Analysis Date = 02/08/15 Pct Recovery = 110% Analysis Date = 02/08/15 Pct Recovery = 110% Analysis Date = 02/03/15 Pct Recovery = 110% Analysis Date = 02/03/15 Pct Recovery = 110% Analysis Date = 01/29/15 Pct Recovery = 110% Analysis Date = 01/29/15 Pct Recovery = 110% Analysis Date = 01/25/15 Pct Recovery = 110% Analysis Date = 01/25/15 Pct Recovery = 110% Analysis Date = 01/20/15 Pct Recovery = 111% Analysis Date = 01/20/15 Pct Recovery = 111% Analysis Date = 01/15/15 Pct Recovery = 111% Analysis Date = 01/15/15 Pct Recovery = 111% Analysis Date = 01/10/15 Pct Recovery = 111% Analysis Date = 01/10/15 Pct Recovery = 111% Analysis Date = 01/06/15 Pct Recovery = 111% Analysis Date = 01/06/15 Pct Recovery = 111% Analysis Date = 01/01/15 Pct Recovery = 111% Analysis Date = 01/01/15 Pct Recovery = 111% Analysis Date = 12/27/14 Pct Recovery = 111% Analysis Date = 12/27/14 Pct Recovery = 111% Analysis Date = 12/22/14 Pct Recovery = 112% Analysis Date = 12/22/14 Pct Recovery = 112% Analysis Date = 12/17/14 Pct Recovery = 112% Analysis Date = 12/17/14 Pct Recovery = 112% Analysis Date = 12/13/14 Pct Recovery = 112% Analysis Date = 12/13/14 Pct Recovery = 112% Analysis Date = 12/08/14 Pct Recovery = 112% Analysis Date = 12/08/14 Pct Recovery = 112% Analysis Date = 12/03/14 Pct Recovery = 112% Analysis Date = 12/03/14 Pct Recovery = 112% Analysis Date = 11/28/14 Pct Recovery = 113% Analysis Date = 11/28/14 Pct Recovery = 113% Analysis Date = 11/24/14 Pct Recovery = 113% Analysis Date = 11/24/14 Pct Recovery = 113% Analysis Date = 11/19/14 Pct Recovery = 113% Analysis Date = 11/19/14 Pct Recovery = 113% Analysis Date = 11/14/14 Pct Recovery = 113% Analysis Date = 11/14/14 Pct Recovery = 113% Analysis Date = 11/09/14 Pct Recovery = 113% Analysis Date = 11/09/14 Pct Recovery = 113% Analysis Date = 11/05/14 Pct Recovery = 114% Analysis Date = 11/05/14 Pct Recovery = 114% Analysis Date = 10/31/14 Pct Recovery = 114% Analysis Date = 10/31/14 Pct Recovery = 114% Analysis Date = 10/26/14 Pct Recovery = 114% Analysis Date = 10/26/14 Pct Recovery = 114% Analysis Date = 10/21/14 Pct Recovery = 114% Analysis Date = 10/21/14 Pct Recovery = 114% Analysis Date = 10/16/14 Pct Recovery = 114% Analysis Date = 10/16/14 Pct Recovery = 114% Analysis Date = 10/12/14 Pct Recovery = 114% Analysis Date = 10/12/14 Pct Recovery = 114% Analysis Date = 10/07/14 Pct Recovery = 115% Analysis Date = 10/07/14 Pct Recovery = 115% Analysis Date = 10/02/14 Pct Recovery = 115% Analysis Date = 10/02/14 Pct Recovery = 115% Analysis Date = 09/27/14 Pct Recovery = 115% Analysis Date = 09/27/14 Pct Recovery = 115% Analysis Date = 09/23/14 Pct Recovery = 115% Analysis Date = 09/23/14 Pct Recovery = 115% Analysis Date = 09/18/14 Pct Recovery = 115% Analysis Date = 09/18/14 Pct Recovery = 115% Analysis Date = 09/13/14 Pct Recovery = 115% Analysis Date = 09/13/14 Pct Recovery = 115% Analysis Date = 09/08/14 Pct Recovery = 116% Analysis Date = 09/08/14 Pct Recovery = 116% Analysis Date = 09/04/14 Pct Recovery = 116% Analysis Date = 09/04/14 Pct Recovery = 116% Analysis Date = 08/30/14 Pct Recovery = 116% Analysis Date = 08/30/14 Pct Recovery = 116% Analysis Date = 08/25/14 Pct Recovery = 116% Analysis Date = 08/25/14 Pct Recovery = 116% Analysis Date = 08/20/14 Pct Recovery = 116% Analysis Date = 08/20/14 Pct Recovery = 116% Analysis Date = 08/15/14 Pct Recovery = 117% Analysis Date = 08/15/14 Pct Recovery = 117% Analysis Date = 08/11/14 Pct Recovery = 117% Analysis Date = 08/11/14 Pct Recovery = 117% Analysis Date = 08/06/14 Pct Recovery = 117% Analysis Date = 08/06/14 Pct Recovery = 117% Analysis Date = 08/01/14 Pct Recovery = 117% Analysis Date = 08/01/14 Pct Recovery = 117% Analysis Date = 07/27/14 Pct Recovery = 117% Analysis Date = 07/27/14 Pct Recovery = 117% Analysis Date = 07/23/14 Pct Recovery = 117% Analysis Date = 07/23/14 Pct Recovery = 117% Analysis Date = 07/18/14 Pct Recovery = 118% Analysis Date = 07/18/14 Pct Recovery = 118% Analysis Date = 07/13/14 Pct Recovery = 118% Analysis Date = 07/13/14 Pct Recovery = 118% Analysis Date = 07/08/14 Pct Recovery = 118% Analysis Date = 07/08/14 Pct Recovery = 118% Analysis Date = 07/04/14 Pct Recovery = 118% Analysis Date = 07/04/14 Pct Recovery = 118% Analysis Date = 06/29/14 Pct Recovery = 118% Analysis Date = 06/29/14 Pct Recovery = 118% Analysis Date = 06/24/14 Pct Recovery = 119% Analysis Date = 06/24/14 Pct Recovery = 119% Analysis Date = 06/19/14 Pct Recovery = 119% Analysis Date = 06/19/14 Pct Recovery = 119% Analysis Date = 06/14/14 Pct Recovery = 119% Analysis Date = 06/14/14 Pct Recovery = 119% Analysis Date = 06/10/14 Pct Recovery = 119% Analysis Date = 06/10/14 Pct Recovery = 119% Analysis Date = 06/05/14 Pct Recovery = 119% Analysis Date = 06/05/14 Pct Recovery = 119% Analysis Date = 05/31/14 Pct Recovery = 119% Analysis Date = 05/31/14 Pct Recovery = 119% Analysis Date = 05/26/14 Pct Recovery = 120% Analysis Date = 05/26/14 Pct Recovery = 120% Analysis Date = 05/22/14 Pct Recovery = 120% Analysis Date = 05/22/14 Pct Recovery = 120% Analysis Date = 05/17/14 Pct Recovery = 120% Analysis Date = 05/17/14 Pct Recovery = 120% Analysis Date = 05/12/14 Pct Recovery = 120% Analysis Date = 05/12/14 Pct Recovery = 120% Analysis Date = 05/07/14 Pct Recovery = 120% Analysis Date = 05/07/14 Pct Recovery = 120% Analysis Date = 05/03/14 Pct Recovery = 120% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
TETRACHLOROETHYLENE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 47 112% 17% 113% 20%
Total 47 112% 17% 113% 20%

Sample Statistics
TETRACHLOROETHYLENE

Characteristic N % % Basis
Plotted 47 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 47 .  
False Negatives 0 0% 0 out of 47
Not Spiked 26 .  
False Positives 5 19% 5 out of 26

BQS OBSP Determination:
TETRACHLOROMETHANE
METHOD: 4440 , TESTIDCODE: 32102GCM66
Open Data Set

Analysis Date = 12/12/16 SpikeMix = Accu 216041125: 40 µl & Crescent 03FF058: 40 µl Pct Recovery = 92% Analysis Date = 07/20/16 SpikeMix = Supelco LC20141V: 40 µl & Accu 216041125: 40 µl Pct Recovery = 89% Analysis Date = 08/12/16 SpikeMix = ChemService 5082900: 25 µl & Phenova B20160319: 25 µl Pct Recovery = 90% Analysis Date = 06/21/16 SpikeMix = Phenova B20160319: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 96% Analysis Date = 09/08/16 SpikeMix = Supelco LC20141V: 25 µl & Accu 216041125: 25 µl Pct Recovery = 82% Analysis Date = 05/24/16 SpikeMix = Accu 216041125: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 83% Analysis Date = 04/09/15 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 102% Analysis Date = 08/19/14 SpikeMix = Spex Organics C1140417015: 20 µl & Accu 214031115: 20 µl Pct Recovery = 96% Analysis Date = 07/01/14 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 103% Analysis Date = 05/01/14 SpikeMix = Accu 214031115: 20 µl & NSI 032614: 20 µl Pct Recovery = 100% Analysis Date = 03/19/15 SpikeMix = Spex Organics C1140417015: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 93% Analysis Date = 12/17/14 SpikeMix = Supelco LC06438: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 84% Analysis Date = 11/14/14 SpikeMix = Crescent 03DD004: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 80% Analysis Date = 06/10/14 SpikeMix = Crescent 03DD004: 20 µl & NSI 032614: 20 µl Pct Recovery = 89% Analysis Date = 09/29/15 SpikeMix = Accu 215041380: 25 µl & ERA 0406-15-03: 25 µl Pct Recovery = 89% Analysis Date = 06/16/15 SpikeMix = ERA 0406-15-03: 25 µl & Supelco LC13545: 25 µl Pct Recovery = 86% Analysis Date = 07/13/15 SpikeMix = Crescent 04EE008: 25 µl & NSI 050515AVOC: 25 µl Pct Recovery = 101% Analysis Date = 11/29/16 SpikeMix = ChemService 5082900: 15 µl & Phenova B20160319: 15 µl Pct Recovery = 92% Analysis Date = 09/08/16 SpikeMix = Phenova B20160319: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 97% Analysis Date = 05/27/16 SpikeMix = Phenova B20160319: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 95% Analysis Date = 08/20/16 SpikeMix = Accu 216041125: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 94% Analysis Date = 06/30/16 SpikeMix = ChemService 5082900: 15 µl & Accu 216041125: 15 µl Pct Recovery = 74% Analysis Date = 04/26/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 92% Analysis Date = 03/04/16 SpikeMix = Accu 215041380: 15 µl & ERA 0406-15-03: 15 µl Pct Recovery = 101% Analysis Date = 02/05/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 87% Analysis Date = 10/16/15 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 89% Analysis Date = 11/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 79% Analysis Date = 10/17/15 SpikeMix = Crescent 04EE008: 15 µl & NSI 050515AVOC: 15 µl Pct Recovery = 91% Analysis Date = 06/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Accu 215041380: 15 µl Pct Recovery = 100% Analysis Date = 01/13/15 SpikeMix = Accu 214031115: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 97% Analysis Date = 09/09/14 SpikeMix = Accu 214031115: 10 µl & NSI 032614: 10 µl Pct Recovery = 97% Analysis Date = 07/23/14 SpikeMix = Spex Organics C1140417015: 10 µl & Accu 214031115: 10 µl Pct Recovery = 121% Analysis Date = 06/18/14 SpikeMix = Supelco LC06438: 10 µl & Accu 214031115: 10 µl Pct Recovery = 115% Analysis Date = 11/06/14 SpikeMix = Spex Organics C1140417015: 10 µl & Crescent 03DD004: 10 µl Pct Recovery = 88% Analysis Date = 10/04/14 SpikeMix = Crescent 03DD004: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 94% Analysis Date = 07/29/14 SpikeMix = Crescent 03DD004: 10 µl & NSI 032614: 10 µl Pct Recovery = 107% Analysis Date = 05/03/14 SpikeMix = Crescent 03DD004: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 98% Analysis Date = 11/20/15 SpikeMix = Accu 215041380: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 95% Analysis Date = 07/31/15 SpikeMix = Crescent 04EE008: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 79% Analysis Date = 06/27/15 SpikeMix = ERA 0406-15-03: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 93% Analysis Date = 03/17/16 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 118% Analysis Date = 01/27/16 SpikeMix = Crescent 04EE008: 10 µl & NSI 050515AVOC: 10 µl Pct Recovery = 103% Analysis Date = 12/10/15 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 108% Analysis Date = 09/03/15 SpikeMix = NSI 050515AVOC: 10 µl & Spex Organics EN150428007: 10 µl Pct Recovery = 93% Analysis Date = 12/11/16 Pct Recovery = 89% Analysis Date = 12/07/16 Pct Recovery = 89% Analysis Date = 12/07/16 Pct Recovery = 89% Analysis Date = 12/02/16 Pct Recovery = 89% Analysis Date = 12/02/16 Pct Recovery = 89% Analysis Date = 11/27/16 Pct Recovery = 89% Analysis Date = 11/27/16 Pct Recovery = 89% Analysis Date = 11/22/16 Pct Recovery = 89% Analysis Date = 11/22/16 Pct Recovery = 89% Analysis Date = 11/18/16 Pct Recovery = 89% Analysis Date = 11/18/16 Pct Recovery = 89% Analysis Date = 11/13/16 Pct Recovery = 89% Analysis Date = 11/13/16 Pct Recovery = 89% Analysis Date = 11/08/16 Pct Recovery = 89% Analysis Date = 11/08/16 Pct Recovery = 89% Analysis Date = 11/03/16 Pct Recovery = 89% Analysis Date = 11/03/16 Pct Recovery = 89% Analysis Date = 10/29/16 Pct Recovery = 89% Analysis Date = 10/29/16 Pct Recovery = 89% Analysis Date = 10/25/16 Pct Recovery = 90% Analysis Date = 10/25/16 Pct Recovery = 90% Analysis Date = 10/20/16 Pct Recovery = 90% Analysis Date = 10/20/16 Pct Recovery = 90% Analysis Date = 10/15/16 Pct Recovery = 90% Analysis Date = 10/15/16 Pct Recovery = 90% Analysis Date = 10/10/16 Pct Recovery = 90% Analysis Date = 10/10/16 Pct Recovery = 90% Analysis Date = 10/06/16 Pct Recovery = 90% Analysis Date = 10/06/16 Pct Recovery = 90% Analysis Date = 10/01/16 Pct Recovery = 90% Analysis Date = 10/01/16 Pct Recovery = 90% Analysis Date = 09/26/16 Pct Recovery = 90% Analysis Date = 09/26/16 Pct Recovery = 90% Analysis Date = 09/21/16 Pct Recovery = 90% Analysis Date = 09/21/16 Pct Recovery = 90% Analysis Date = 09/16/16 Pct Recovery = 90% Analysis Date = 09/16/16 Pct Recovery = 90% Analysis Date = 09/12/16 Pct Recovery = 91% Analysis Date = 09/12/16 Pct Recovery = 91% Analysis Date = 09/07/16 Pct Recovery = 91% Analysis Date = 09/07/16 Pct Recovery = 91% Analysis Date = 09/02/16 Pct Recovery = 91% Analysis Date = 09/02/16 Pct Recovery = 91% Analysis Date = 08/28/16 Pct Recovery = 91% Analysis Date = 08/28/16 Pct Recovery = 91% Analysis Date = 08/24/16 Pct Recovery = 91% Analysis Date = 08/24/16 Pct Recovery = 91% Analysis Date = 08/19/16 Pct Recovery = 91% Analysis Date = 08/19/16 Pct Recovery = 91% Analysis Date = 08/14/16 Pct Recovery = 91% Analysis Date = 08/14/16 Pct Recovery = 91% Analysis Date = 08/09/16 Pct Recovery = 91% Analysis Date = 08/09/16 Pct Recovery = 91% Analysis Date = 08/04/16 Pct Recovery = 91% Analysis Date = 08/04/16 Pct Recovery = 91% Analysis Date = 07/31/16 Pct Recovery = 91% Analysis Date = 07/31/16 Pct Recovery = 91% Analysis Date = 07/26/16 Pct Recovery = 92% Analysis Date = 07/26/16 Pct Recovery = 92% Analysis Date = 07/21/16 Pct Recovery = 92% Analysis Date = 07/21/16 Pct Recovery = 92% Analysis Date = 07/16/16 Pct Recovery = 92% Analysis Date = 07/16/16 Pct Recovery = 92% Analysis Date = 07/12/16 Pct Recovery = 92% Analysis Date = 07/12/16 Pct Recovery = 92% Analysis Date = 07/07/16 Pct Recovery = 92% Analysis Date = 07/07/16 Pct Recovery = 92% Analysis Date = 07/02/16 Pct Recovery = 92% Analysis Date = 07/02/16 Pct Recovery = 92% Analysis Date = 06/27/16 Pct Recovery = 92% Analysis Date = 06/27/16 Pct Recovery = 92% Analysis Date = 06/22/16 Pct Recovery = 92% Analysis Date = 06/22/16 Pct Recovery = 92% Analysis Date = 06/18/16 Pct Recovery = 92% Analysis Date = 06/18/16 Pct Recovery = 92% Analysis Date = 06/13/16 Pct Recovery = 92% Analysis Date = 06/13/16 Pct Recovery = 92% Analysis Date = 06/08/16 Pct Recovery = 92% Analysis Date = 06/08/16 Pct Recovery = 92% Analysis Date = 06/03/16 Pct Recovery = 92% Analysis Date = 06/03/16 Pct Recovery = 92% Analysis Date = 05/30/16 Pct Recovery = 93% Analysis Date = 05/30/16 Pct Recovery = 93% Analysis Date = 05/25/16 Pct Recovery = 93% Analysis Date = 05/25/16 Pct Recovery = 93% Analysis Date = 05/20/16 Pct Recovery = 93% Analysis Date = 05/20/16 Pct Recovery = 93% Analysis Date = 05/15/16 Pct Recovery = 93% Analysis Date = 05/15/16 Pct Recovery = 93% Analysis Date = 05/10/16 Pct Recovery = 93% Analysis Date = 05/10/16 Pct Recovery = 93% Analysis Date = 05/06/16 Pct Recovery = 93% Analysis Date = 05/06/16 Pct Recovery = 93% Analysis Date = 05/01/16 Pct Recovery = 93% Analysis Date = 05/01/16 Pct Recovery = 93% Analysis Date = 04/26/16 Pct Recovery = 93% Analysis Date = 04/26/16 Pct Recovery = 93% Analysis Date = 04/21/16 Pct Recovery = 93% Analysis Date = 04/21/16 Pct Recovery = 93% Analysis Date = 04/16/16 Pct Recovery = 93% Analysis Date = 04/16/16 Pct Recovery = 93% Analysis Date = 04/12/16 Pct Recovery = 93% Analysis Date = 04/12/16 Pct Recovery = 93% Analysis Date = 04/07/16 Pct Recovery = 93% Analysis Date = 04/07/16 Pct Recovery = 93% Analysis Date = 04/02/16 Pct Recovery = 93% Analysis Date = 04/02/16 Pct Recovery = 93% Analysis Date = 03/28/16 Pct Recovery = 93% Analysis Date = 03/28/16 Pct Recovery = 93% Analysis Date = 03/24/16 Pct Recovery = 93% Analysis Date = 03/24/16 Pct Recovery = 93% Analysis Date = 03/19/16 Pct Recovery = 93% Analysis Date = 03/19/16 Pct Recovery = 93% Analysis Date = 03/14/16 Pct Recovery = 93% Analysis Date = 03/14/16 Pct Recovery = 93% Analysis Date = 03/09/16 Pct Recovery = 93% Analysis Date = 03/09/16 Pct Recovery = 93% Analysis Date = 03/04/16 Pct Recovery = 93% Analysis Date = 03/04/16 Pct Recovery = 93% Analysis Date = 02/29/16 Pct Recovery = 93% Analysis Date = 02/29/16 Pct Recovery = 93% Analysis Date = 02/24/16 Pct Recovery = 94% Analysis Date = 02/24/16 Pct Recovery = 94% Analysis Date = 02/19/16 Pct Recovery = 94% Analysis Date = 02/19/16 Pct Recovery = 94% Analysis Date = 02/14/16 Pct Recovery = 94% Analysis Date = 02/14/16 Pct Recovery = 94% Analysis Date = 02/10/16 Pct Recovery = 94% Analysis Date = 02/10/16 Pct Recovery = 94% Analysis Date = 02/05/16 Pct Recovery = 94% Analysis Date = 02/05/16 Pct Recovery = 94% Analysis Date = 01/31/16 Pct Recovery = 94% Analysis Date = 01/31/16 Pct Recovery = 94% Analysis Date = 01/26/16 Pct Recovery = 94% Analysis Date = 01/26/16 Pct Recovery = 94% Analysis Date = 01/21/16 Pct Recovery = 94% Analysis Date = 01/21/16 Pct Recovery = 94% Analysis Date = 01/17/16 Pct Recovery = 94% Analysis Date = 01/17/16 Pct Recovery = 94% Analysis Date = 01/12/16 Pct Recovery = 94% Analysis Date = 01/12/16 Pct Recovery = 94% Analysis Date = 01/07/16 Pct Recovery = 94% Analysis Date = 01/07/16 Pct Recovery = 94% Analysis Date = 01/02/16 Pct Recovery = 94% Analysis Date = 01/02/16 Pct Recovery = 94% Analysis Date = 12/29/15 Pct Recovery = 94% Analysis Date = 12/29/15 Pct Recovery = 94% Analysis Date = 12/24/15 Pct Recovery = 94% Analysis Date = 12/24/15 Pct Recovery = 94% Analysis Date = 12/19/15 Pct Recovery = 94% Analysis Date = 12/19/15 Pct Recovery = 94% Analysis Date = 12/14/15 Pct Recovery = 94% Analysis Date = 12/14/15 Pct Recovery = 94% Analysis Date = 12/09/15 Pct Recovery = 94% Analysis Date = 12/09/15 Pct Recovery = 94% Analysis Date = 12/05/15 Pct Recovery = 94% Analysis Date = 12/05/15 Pct Recovery = 94% Analysis Date = 11/30/15 Pct Recovery = 94% Analysis Date = 11/30/15 Pct Recovery = 94% Analysis Date = 11/25/15 Pct Recovery = 94% Analysis Date = 11/25/15 Pct Recovery = 94% Analysis Date = 11/20/15 Pct Recovery = 94% Analysis Date = 11/20/15 Pct Recovery = 94% Analysis Date = 11/16/15 Pct Recovery = 94% Analysis Date = 11/16/15 Pct Recovery = 94% Analysis Date = 11/11/15 Pct Recovery = 94% Analysis Date = 11/11/15 Pct Recovery = 94% Analysis Date = 11/06/15 Pct Recovery = 94% Analysis Date = 11/06/15 Pct Recovery = 94% Analysis Date = 11/01/15 Pct Recovery = 94% Analysis Date = 11/01/15 Pct Recovery = 94% Analysis Date = 10/27/15 Pct Recovery = 94% Analysis Date = 10/27/15 Pct Recovery = 94% Analysis Date = 10/23/15 Pct Recovery = 94% Analysis Date = 10/23/15 Pct Recovery = 94% Analysis Date = 10/18/15 Pct Recovery = 94% Analysis Date = 10/18/15 Pct Recovery = 94% Analysis Date = 10/13/15 Pct Recovery = 94% Analysis Date = 10/13/15 Pct Recovery = 94% Analysis Date = 10/08/15 Pct Recovery = 94% Analysis Date = 10/08/15 Pct Recovery = 94% Analysis Date = 10/04/15 Pct Recovery = 94% Analysis Date = 10/04/15 Pct Recovery = 94% Analysis Date = 09/29/15 Pct Recovery = 94% Analysis Date = 09/29/15 Pct Recovery = 94% Analysis Date = 09/24/15 Pct Recovery = 94% Analysis Date = 09/24/15 Pct Recovery = 94% Analysis Date = 09/19/15 Pct Recovery = 93% Analysis Date = 09/19/15 Pct Recovery = 93% Analysis Date = 09/14/15 Pct Recovery = 93% Analysis Date = 09/14/15 Pct Recovery = 93% Analysis Date = 09/10/15 Pct Recovery = 93% Analysis Date = 09/10/15 Pct Recovery = 93% Analysis Date = 09/05/15 Pct Recovery = 93% Analysis Date = 09/05/15 Pct Recovery = 93% Analysis Date = 08/31/15 Pct Recovery = 93% Analysis Date = 08/31/15 Pct Recovery = 93% Analysis Date = 08/26/15 Pct Recovery = 93% Analysis Date = 08/26/15 Pct Recovery = 93% Analysis Date = 08/21/15 Pct Recovery = 93% Analysis Date = 08/21/15 Pct Recovery = 93% Analysis Date = 08/17/15 Pct Recovery = 93% Analysis Date = 08/17/15 Pct Recovery = 93% Analysis Date = 08/12/15 Pct Recovery = 93% Analysis Date = 08/12/15 Pct Recovery = 93% Analysis Date = 08/07/15 Pct Recovery = 93% Analysis Date = 08/07/15 Pct Recovery = 93% Analysis Date = 08/02/15 Pct Recovery = 93% Analysis Date = 08/02/15 Pct Recovery = 93% Analysis Date = 07/29/15 Pct Recovery = 93% Analysis Date = 07/29/15 Pct Recovery = 93% Analysis Date = 07/24/15 Pct Recovery = 93% Analysis Date = 07/24/15 Pct Recovery = 93% Analysis Date = 07/19/15 Pct Recovery = 93% Analysis Date = 07/19/15 Pct Recovery = 93% Analysis Date = 07/14/15 Pct Recovery = 93% Analysis Date = 07/14/15 Pct Recovery = 93% Analysis Date = 07/09/15 Pct Recovery = 92% Analysis Date = 07/09/15 Pct Recovery = 92% Analysis Date = 07/05/15 Pct Recovery = 92% Analysis Date = 07/05/15 Pct Recovery = 92% Analysis Date = 06/30/15 Pct Recovery = 92% Analysis Date = 06/30/15 Pct Recovery = 92% Analysis Date = 06/25/15 Pct Recovery = 92% Analysis Date = 06/25/15 Pct Recovery = 92% Analysis Date = 06/20/15 Pct Recovery = 92% Analysis Date = 06/20/15 Pct Recovery = 92% Analysis Date = 06/16/15 Pct Recovery = 92% Analysis Date = 06/16/15 Pct Recovery = 92% Analysis Date = 06/11/15 Pct Recovery = 92% Analysis Date = 06/11/15 Pct Recovery = 92% Analysis Date = 06/06/15 Pct Recovery = 92% Analysis Date = 06/06/15 Pct Recovery = 92% Analysis Date = 06/01/15 Pct Recovery = 92% Analysis Date = 06/01/15 Pct Recovery = 92% Analysis Date = 05/27/15 Pct Recovery = 92% Analysis Date = 05/27/15 Pct Recovery = 92% Analysis Date = 05/23/15 Pct Recovery = 92% Analysis Date = 05/23/15 Pct Recovery = 92% Analysis Date = 05/18/15 Pct Recovery = 92% Analysis Date = 05/18/15 Pct Recovery = 92% Analysis Date = 05/13/15 Pct Recovery = 92% Analysis Date = 05/13/15 Pct Recovery = 92% Analysis Date = 05/08/15 Pct Recovery = 92% Analysis Date = 05/08/15 Pct Recovery = 92% Analysis Date = 05/04/15 Pct Recovery = 92% Analysis Date = 05/04/15 Pct Recovery = 92% Analysis Date = 04/29/15 Pct Recovery = 93% Analysis Date = 04/29/15 Pct Recovery = 93% Analysis Date = 04/24/15 Pct Recovery = 93% Analysis Date = 04/24/15 Pct Recovery = 93% Analysis Date = 04/19/15 Pct Recovery = 93% Analysis Date = 04/19/15 Pct Recovery = 93% Analysis Date = 04/14/15 Pct Recovery = 93% Analysis Date = 04/14/15 Pct Recovery = 93% Analysis Date = 04/10/15 Pct Recovery = 93% Analysis Date = 04/10/15 Pct Recovery = 93% Analysis Date = 04/05/15 Pct Recovery = 93% Analysis Date = 04/05/15 Pct Recovery = 93% Analysis Date = 03/31/15 Pct Recovery = 93% Analysis Date = 03/31/15 Pct Recovery = 93% Analysis Date = 03/26/15 Pct Recovery = 93% Analysis Date = 03/26/15 Pct Recovery = 93% Analysis Date = 03/22/15 Pct Recovery = 93% Analysis Date = 03/22/15 Pct Recovery = 93% Analysis Date = 03/17/15 Pct Recovery = 93% Analysis Date = 03/17/15 Pct Recovery = 93% Analysis Date = 03/12/15 Pct Recovery = 93% Analysis Date = 03/12/15 Pct Recovery = 93% Analysis Date = 03/07/15 Pct Recovery = 93% Analysis Date = 03/07/15 Pct Recovery = 93% Analysis Date = 03/02/15 Pct Recovery = 93% Analysis Date = 03/02/15 Pct Recovery = 93% Analysis Date = 02/26/15 Pct Recovery = 94% Analysis Date = 02/26/15 Pct Recovery = 94% Analysis Date = 02/21/15 Pct Recovery = 94% Analysis Date = 02/21/15 Pct Recovery = 94% Analysis Date = 02/16/15 Pct Recovery = 94% Analysis Date = 02/16/15 Pct Recovery = 94% Analysis Date = 02/11/15 Pct Recovery = 94% Analysis Date = 02/11/15 Pct Recovery = 94% Analysis Date = 02/07/15 Pct Recovery = 94% Analysis Date = 02/07/15 Pct Recovery = 94% Analysis Date = 02/02/15 Pct Recovery = 94% Analysis Date = 02/02/15 Pct Recovery = 94% Analysis Date = 01/28/15 Pct Recovery = 94% Analysis Date = 01/28/15 Pct Recovery = 94% Analysis Date = 01/23/15 Pct Recovery = 94% Analysis Date = 01/23/15 Pct Recovery = 94% Analysis Date = 01/18/15 Pct Recovery = 94% Analysis Date = 01/18/15 Pct Recovery = 94% Analysis Date = 01/14/15 Pct Recovery = 94% Analysis Date = 01/14/15 Pct Recovery = 94% Analysis Date = 01/09/15 Pct Recovery = 94% Analysis Date = 01/09/15 Pct Recovery = 94% Analysis Date = 01/04/15 Pct Recovery = 95% Analysis Date = 01/04/15 Pct Recovery = 95% Analysis Date = 12/30/14 Pct Recovery = 95% Analysis Date = 12/30/14 Pct Recovery = 95% Analysis Date = 12/25/14 Pct Recovery = 95% Analysis Date = 12/25/14 Pct Recovery = 95% Analysis Date = 12/21/14 Pct Recovery = 95% Analysis Date = 12/21/14 Pct Recovery = 95% Analysis Date = 12/16/14 Pct Recovery = 95% Analysis Date = 12/16/14 Pct Recovery = 95% Analysis Date = 12/11/14 Pct Recovery = 95% Analysis Date = 12/11/14 Pct Recovery = 95% Analysis Date = 12/06/14 Pct Recovery = 95% Analysis Date = 12/06/14 Pct Recovery = 95% Analysis Date = 12/02/14 Pct Recovery = 96% Analysis Date = 12/02/14 Pct Recovery = 96% Analysis Date = 11/27/14 Pct Recovery = 96% Analysis Date = 11/27/14 Pct Recovery = 96% Analysis Date = 11/22/14 Pct Recovery = 96% Analysis Date = 11/22/14 Pct Recovery = 96% Analysis Date = 11/17/14 Pct Recovery = 96% Analysis Date = 11/17/14 Pct Recovery = 96% Analysis Date = 11/12/14 Pct Recovery = 96% Analysis Date = 11/12/14 Pct Recovery = 96% Analysis Date = 11/08/14 Pct Recovery = 96% Analysis Date = 11/08/14 Pct Recovery = 96% Analysis Date = 11/03/14 Pct Recovery = 97% Analysis Date = 11/03/14 Pct Recovery = 97% Analysis Date = 10/29/14 Pct Recovery = 97% Analysis Date = 10/29/14 Pct Recovery = 97% Analysis Date = 10/24/14 Pct Recovery = 97% Analysis Date = 10/24/14 Pct Recovery = 97% Analysis Date = 10/20/14 Pct Recovery = 97% Analysis Date = 10/20/14 Pct Recovery = 97% Analysis Date = 10/15/14 Pct Recovery = 97% Analysis Date = 10/15/14 Pct Recovery = 97% Analysis Date = 10/10/14 Pct Recovery = 97% Analysis Date = 10/10/14 Pct Recovery = 97% Analysis Date = 10/05/14 Pct Recovery = 97% Analysis Date = 10/05/14 Pct Recovery = 97% Analysis Date = 09/30/14 Pct Recovery = 98% Analysis Date = 09/30/14 Pct Recovery = 98% Analysis Date = 09/26/14 Pct Recovery = 98% Analysis Date = 09/26/14 Pct Recovery = 98% Analysis Date = 09/21/14 Pct Recovery = 98% Analysis Date = 09/21/14 Pct Recovery = 98% Analysis Date = 09/16/14 Pct Recovery = 98% Analysis Date = 09/16/14 Pct Recovery = 98% Analysis Date = 09/11/14 Pct Recovery = 98% Analysis Date = 09/11/14 Pct Recovery = 98% Analysis Date = 09/07/14 Pct Recovery = 98% Analysis Date = 09/07/14 Pct Recovery = 98% Analysis Date = 09/02/14 Pct Recovery = 98% Analysis Date = 09/02/14 Pct Recovery = 98% Analysis Date = 08/28/14 Pct Recovery = 99% Analysis Date = 08/28/14 Pct Recovery = 99% Analysis Date = 08/23/14 Pct Recovery = 99% Analysis Date = 08/23/14 Pct Recovery = 99% Analysis Date = 08/18/14 Pct Recovery = 99% Analysis Date = 08/18/14 Pct Recovery = 99% Analysis Date = 08/14/14 Pct Recovery = 99% Analysis Date = 08/14/14 Pct Recovery = 99% Analysis Date = 08/09/14 Pct Recovery = 99% Analysis Date = 08/09/14 Pct Recovery = 99% Analysis Date = 08/04/14 Pct Recovery = 99% Analysis Date = 08/04/14 Pct Recovery = 99% Analysis Date = 07/30/14 Pct Recovery = 99% Analysis Date = 07/30/14 Pct Recovery = 99% Analysis Date = 07/26/14 Pct Recovery = 100% Analysis Date = 07/26/14 Pct Recovery = 100% Analysis Date = 07/21/14 Pct Recovery = 100% Analysis Date = 07/21/14 Pct Recovery = 100% Analysis Date = 07/16/14 Pct Recovery = 100% Analysis Date = 07/16/14 Pct Recovery = 100% Analysis Date = 07/11/14 Pct Recovery = 100% Analysis Date = 07/11/14 Pct Recovery = 100% Analysis Date = 07/06/14 Pct Recovery = 100% Analysis Date = 07/06/14 Pct Recovery = 100% Analysis Date = 07/02/14 Pct Recovery = 100% Analysis Date = 07/02/14 Pct Recovery = 100% Analysis Date = 06/27/14 Pct Recovery = 101% Analysis Date = 06/27/14 Pct Recovery = 101% Analysis Date = 06/22/14 Pct Recovery = 101% Analysis Date = 06/22/14 Pct Recovery = 101% Analysis Date = 06/17/14 Pct Recovery = 101% Analysis Date = 06/17/14 Pct Recovery = 101% Analysis Date = 06/13/14 Pct Recovery = 101% Analysis Date = 06/13/14 Pct Recovery = 101% Analysis Date = 06/08/14 Pct Recovery = 101% Analysis Date = 06/08/14 Pct Recovery = 101% Analysis Date = 06/03/14 Pct Recovery = 101% Analysis Date = 06/03/14 Pct Recovery = 101% Analysis Date = 05/29/14 Pct Recovery = 102% Analysis Date = 05/29/14 Pct Recovery = 102% Analysis Date = 05/24/14 Pct Recovery = 102% Analysis Date = 05/24/14 Pct Recovery = 102% Analysis Date = 05/20/14 Pct Recovery = 102% Analysis Date = 05/20/14 Pct Recovery = 102% Analysis Date = 05/15/14 Pct Recovery = 102% Analysis Date = 05/15/14 Pct Recovery = 102% Analysis Date = 05/10/14 Pct Recovery = 102% Analysis Date = 05/10/14 Pct Recovery = 102% Analysis Date = 05/05/14 Pct Recovery = 103% Analysis Date = 05/05/14 Pct Recovery = 103% Analysis Date = 05/01/14 Pct Recovery = 103% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
TETRACHLOROMETHANE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 44 94% 10% 94% 8%
Total 44 94% 10% 94% 8%

Sample Statistics
TETRACHLOROMETHANE

Characteristic N % % Basis
Plotted 44 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 44 .  
False Negatives 0 0% 0 out of 44
Not Spiked 22 .  
False Positives 0 0% 0 out of 22

BQS OBSP Determination:
TETRAHYDROFURAN
METHOD: 4440 , TESTIDCODE: 81607GCM66
Open Data Set

Analysis Date = 12/16/16 SpikeMix = NSI 041816AVOC: 40 µl & ChemService 5082900: 40 µl Pct Recovery = 113% Analysis Date = 07/14/16 SpikeMix = Accu 216041125: 40 µl & NSI 041816AVOC: 40 µl Pct Recovery = 109% Analysis Date = 12/12/16 SpikeMix = Accu 216041125: 40 µl & Crescent 03FF058: 40 µl Pct Recovery = 110% Analysis Date = 08/04/16 SpikeMix = Crescent 03FF058: 40 µl & Supelco LC20141V: 40 µl Pct Recovery = 102% Analysis Date = 08/26/16 SpikeMix = NSI 041816AVOC: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 108% Analysis Date = 11/21/16 SpikeMix = Crescent 03FF058: 25 µl & Supelco LC20141V: 25 µl Pct Recovery = 100% Analysis Date = 06/30/16 SpikeMix = Crescent 03FF058: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 105% Analysis Date = 06/21/16 SpikeMix = Phenova B20160319: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 108% Analysis Date = 05/24/16 SpikeMix = Accu 216041125: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 104% Analysis Date = 08/15/15 SpikeMix = Supelco LC13545: 25 µl & Crescent 04EE008: 25 µl Pct Recovery = 101% Analysis Date = 06/16/15 SpikeMix = ERA 0406-15-03: 25 µl & Supelco LC13545: 25 µl Pct Recovery = 93% Analysis Date = 10/13/16 SpikeMix = Accu 216041125: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 103% Analysis Date = 10/13/16 SpikeMix = NSI 041816AVOC: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 102% Analysis Date = 07/29/16 SpikeMix = Phenova B20160319: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 102% Analysis Date = 06/10/16 SpikeMix = NSI 041816AVOC: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 112% Analysis Date = 09/28/16 SpikeMix = Crescent 03FF058: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 91% Analysis Date = 09/08/16 SpikeMix = Phenova B20160319: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 108% Analysis Date = 08/20/16 SpikeMix = Accu 216041125: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 109% Analysis Date = 04/09/15 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 88% Analysis Date = 08/19/14 SpikeMix = Spex Organics C1140417015: 20 µl & Accu 214031115: 20 µl Pct Recovery = 89% Analysis Date = 07/01/14 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 99% Analysis Date = 05/01/14 SpikeMix = Accu 214031115: 20 µl & NSI 032614: 20 µl Pct Recovery = 85% Analysis Date = 03/19/15 SpikeMix = Spex Organics C1140417015: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 86% Analysis Date = 12/17/14 SpikeMix = Supelco LC06438: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 78% Analysis Date = 11/14/14 SpikeMix = Crescent 03DD004: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 81% Analysis Date = 06/10/14 SpikeMix = Crescent 03DD004: 20 µl & NSI 032614: 20 µl Pct Recovery = 83% Analysis Date = 04/26/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 120% Analysis Date = 02/05/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 86% Analysis Date = 11/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 101% Analysis Date = 10/16/15 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 100% Analysis Date = 05/09/15 SpikeMix = Spex Organics EN150428007: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 103% Analysis Date = 04/02/16 SpikeMix = Supelco LC13545: 15 µl & Accu 215041380: 15 µl Pct Recovery = 106% Analysis Date = 12/18/15 SpikeMix = Supelco LC13545: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 103% Analysis Date = 02/18/16 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 100% Analysis Date = 11/12/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 95% Analysis Date = 09/03/15 SpikeMix = NSI 050515AVOC: 10 µl & Spex Organics EN150428007: 10 µl Pct Recovery = 88% Analysis Date = 05/21/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 106% Analysis Date = 05/13/16 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 102% Analysis Date = 03/17/16 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 95% Analysis Date = 12/10/15 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 98% Analysis Date = 06/27/15 SpikeMix = ERA 0406-15-03: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 90% Analysis Date = 05/09/15 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 95% Analysis Date = 01/13/15 SpikeMix = Accu 214031115: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 89% Analysis Date = 09/09/14 SpikeMix = Accu 214031115: 10 µl & NSI 032614: 10 µl Pct Recovery = 107% Analysis Date = 07/23/14 SpikeMix = Spex Organics C1140417015: 10 µl & Accu 214031115: 10 µl Pct Recovery = 105% Analysis Date = 06/18/14 SpikeMix = Supelco LC06438: 10 µl & Accu 214031115: 10 µl Pct Recovery = 125% Analysis Date = 11/06/14 SpikeMix = Spex Organics C1140417015: 10 µl & Crescent 03DD004: 10 µl Pct Recovery = 86% Analysis Date = 10/04/14 SpikeMix = Crescent 03DD004: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 87% Analysis Date = 07/29/14 SpikeMix = Crescent 03DD004: 10 µl & NSI 032614: 10 µl Pct Recovery = 77% Analysis Date = 05/03/14 SpikeMix = Crescent 03DD004: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 82% Analysis Date = 12/15/16 Pct Recovery = 107% Analysis Date = 12/11/16 Pct Recovery = 107% Analysis Date = 12/11/16 Pct Recovery = 107% Analysis Date = 12/06/16 Pct Recovery = 107% Analysis Date = 12/06/16 Pct Recovery = 107% Analysis Date = 12/01/16 Pct Recovery = 107% Analysis Date = 12/01/16 Pct Recovery = 107% Analysis Date = 11/26/16 Pct Recovery = 107% Analysis Date = 11/26/16 Pct Recovery = 107% Analysis Date = 11/21/16 Pct Recovery = 107% Analysis Date = 11/21/16 Pct Recovery = 107% Analysis Date = 11/17/16 Pct Recovery = 107% Analysis Date = 11/17/16 Pct Recovery = 107% Analysis Date = 11/12/16 Pct Recovery = 107% Analysis Date = 11/12/16 Pct Recovery = 107% Analysis Date = 11/07/16 Pct Recovery = 106% Analysis Date = 11/07/16 Pct Recovery = 106% Analysis Date = 11/02/16 Pct Recovery = 106% Analysis Date = 11/02/16 Pct Recovery = 106% Analysis Date = 10/28/16 Pct Recovery = 106% Analysis Date = 10/28/16 Pct Recovery = 106% Analysis Date = 10/24/16 Pct Recovery = 106% Analysis Date = 10/24/16 Pct Recovery = 106% Analysis Date = 10/19/16 Pct Recovery = 106% Analysis Date = 10/19/16 Pct Recovery = 106% Analysis Date = 10/14/16 Pct Recovery = 106% Analysis Date = 10/14/16 Pct Recovery = 106% Analysis Date = 10/09/16 Pct Recovery = 106% Analysis Date = 10/09/16 Pct Recovery = 106% Analysis Date = 10/04/16 Pct Recovery = 106% Analysis Date = 10/04/16 Pct Recovery = 106% Analysis Date = 09/30/16 Pct Recovery = 106% Analysis Date = 09/30/16 Pct Recovery = 106% Analysis Date = 09/25/16 Pct Recovery = 106% Analysis Date = 09/25/16 Pct Recovery = 106% Analysis Date = 09/20/16 Pct Recovery = 106% Analysis Date = 09/20/16 Pct Recovery = 106% Analysis Date = 09/15/16 Pct Recovery = 106% Analysis Date = 09/15/16 Pct Recovery = 106% Analysis Date = 09/10/16 Pct Recovery = 106% Analysis Date = 09/10/16 Pct Recovery = 106% Analysis Date = 09/06/16 Pct Recovery = 105% Analysis Date = 09/06/16 Pct Recovery = 105% Analysis Date = 09/01/16 Pct Recovery = 105% Analysis Date = 09/01/16 Pct Recovery = 105% Analysis Date = 08/27/16 Pct Recovery = 105% Analysis Date = 08/27/16 Pct Recovery = 105% Analysis Date = 08/22/16 Pct Recovery = 105% Analysis Date = 08/22/16 Pct Recovery = 105% Analysis Date = 08/17/16 Pct Recovery = 105% Analysis Date = 08/17/16 Pct Recovery = 105% Analysis Date = 08/13/16 Pct Recovery = 105% Analysis Date = 08/13/16 Pct Recovery = 105% Analysis Date = 08/08/16 Pct Recovery = 105% Analysis Date = 08/08/16 Pct Recovery = 105% Analysis Date = 08/03/16 Pct Recovery = 105% Analysis Date = 08/03/16 Pct Recovery = 105% Analysis Date = 07/29/16 Pct Recovery = 105% Analysis Date = 07/29/16 Pct Recovery = 105% Analysis Date = 07/24/16 Pct Recovery = 105% Analysis Date = 07/24/16 Pct Recovery = 105% Analysis Date = 07/20/16 Pct Recovery = 104% Analysis Date = 07/20/16 Pct Recovery = 104% Analysis Date = 07/15/16 Pct Recovery = 104% Analysis Date = 07/15/16 Pct Recovery = 104% Analysis Date = 07/10/16 Pct Recovery = 104% Analysis Date = 07/10/16 Pct Recovery = 104% Analysis Date = 07/05/16 Pct Recovery = 104% Analysis Date = 07/05/16 Pct Recovery = 104% Analysis Date = 06/30/16 Pct Recovery = 104% Analysis Date = 06/30/16 Pct Recovery = 104% Analysis Date = 06/26/16 Pct Recovery = 104% Analysis Date = 06/26/16 Pct Recovery = 104% Analysis Date = 06/21/16 Pct Recovery = 104% Analysis Date = 06/21/16 Pct Recovery = 104% Analysis Date = 06/16/16 Pct Recovery = 104% Analysis Date = 06/16/16 Pct Recovery = 104% Analysis Date = 06/11/16 Pct Recovery = 104% Analysis Date = 06/11/16 Pct Recovery = 104% Analysis Date = 06/06/16 Pct Recovery = 104% Analysis Date = 06/06/16 Pct Recovery = 104% Analysis Date = 06/02/16 Pct Recovery = 104% Analysis Date = 06/02/16 Pct Recovery = 104% Analysis Date = 05/28/16 Pct Recovery = 103% Analysis Date = 05/28/16 Pct Recovery = 103% Analysis Date = 05/23/16 Pct Recovery = 103% Analysis Date = 05/23/16 Pct Recovery = 103% Analysis Date = 05/18/16 Pct Recovery = 103% Analysis Date = 05/18/16 Pct Recovery = 103% Analysis Date = 05/13/16 Pct Recovery = 103% Analysis Date = 05/13/16 Pct Recovery = 103% Analysis Date = 05/09/16 Pct Recovery = 103% Analysis Date = 05/09/16 Pct Recovery = 103% Analysis Date = 05/04/16 Pct Recovery = 103% Analysis Date = 05/04/16 Pct Recovery = 103% Analysis Date = 04/29/16 Pct Recovery = 103% Analysis Date = 04/29/16 Pct Recovery = 103% Analysis Date = 04/24/16 Pct Recovery = 103% Analysis Date = 04/24/16 Pct Recovery = 103% Analysis Date = 04/19/16 Pct Recovery = 103% Analysis Date = 04/19/16 Pct Recovery = 103% Analysis Date = 04/15/16 Pct Recovery = 103% Analysis Date = 04/15/16 Pct Recovery = 103% Analysis Date = 04/10/16 Pct Recovery = 103% Analysis Date = 04/10/16 Pct Recovery = 103% Analysis Date = 04/05/16 Pct Recovery = 102% Analysis Date = 04/05/16 Pct Recovery = 102% Analysis Date = 03/31/16 Pct Recovery = 102% Analysis Date = 03/31/16 Pct Recovery = 102% Analysis Date = 03/26/16 Pct Recovery = 102% Analysis Date = 03/26/16 Pct Recovery = 102% Analysis Date = 03/22/16 Pct Recovery = 102% Analysis Date = 03/22/16 Pct Recovery = 102% Analysis Date = 03/17/16 Pct Recovery = 102% Analysis Date = 03/17/16 Pct Recovery = 102% Analysis Date = 03/12/16 Pct Recovery = 102% Analysis Date = 03/12/16 Pct Recovery = 102% Analysis Date = 03/07/16 Pct Recovery = 102% Analysis Date = 03/07/16 Pct Recovery = 102% Analysis Date = 03/02/16 Pct Recovery = 101% Analysis Date = 03/02/16 Pct Recovery = 101% Analysis Date = 02/27/16 Pct Recovery = 101% Analysis Date = 02/27/16 Pct Recovery = 101% Analysis Date = 02/22/16 Pct Recovery = 101% Analysis Date = 02/22/16 Pct Recovery = 101% Analysis Date = 02/17/16 Pct Recovery = 101% Analysis Date = 02/17/16 Pct Recovery = 101% Analysis Date = 02/12/16 Pct Recovery = 101% Analysis Date = 02/12/16 Pct Recovery = 101% Analysis Date = 02/07/16 Pct Recovery = 101% Analysis Date = 02/07/16 Pct Recovery = 101% Analysis Date = 02/03/16 Pct Recovery = 101% Analysis Date = 02/03/16 Pct Recovery = 101% Analysis Date = 01/29/16 Pct Recovery = 101% Analysis Date = 01/29/16 Pct Recovery = 101% Analysis Date = 01/24/16 Pct Recovery = 100% Analysis Date = 01/24/16 Pct Recovery = 100% Analysis Date = 01/19/16 Pct Recovery = 100% Analysis Date = 01/19/16 Pct Recovery = 100% Analysis Date = 01/14/16 Pct Recovery = 100% Analysis Date = 01/14/16 Pct Recovery = 100% Analysis Date = 01/10/16 Pct Recovery = 100% Analysis Date = 01/10/16 Pct Recovery = 100% Analysis Date = 01/05/16 Pct Recovery = 100% Analysis Date = 01/05/16 Pct Recovery = 100% Analysis Date = 12/31/15 Pct Recovery = 100% Analysis Date = 12/31/15 Pct Recovery = 100% Analysis Date = 12/26/15 Pct Recovery = 100% Analysis Date = 12/26/15 Pct Recovery = 100% Analysis Date = 12/21/15 Pct Recovery = 100% Analysis Date = 12/21/15 Pct Recovery = 100% Analysis Date = 12/17/15 Pct Recovery = 99% Analysis Date = 12/17/15 Pct Recovery = 99% Analysis Date = 12/12/15 Pct Recovery = 99% Analysis Date = 12/12/15 Pct Recovery = 99% Analysis Date = 12/07/15 Pct Recovery = 99% Analysis Date = 12/07/15 Pct Recovery = 99% Analysis Date = 12/02/15 Pct Recovery = 99% Analysis Date = 12/02/15 Pct Recovery = 99% Analysis Date = 11/27/15 Pct Recovery = 99% Analysis Date = 11/27/15 Pct Recovery = 99% Analysis Date = 11/23/15 Pct Recovery = 99% Analysis Date = 11/23/15 Pct Recovery = 99% Analysis Date = 11/18/15 Pct Recovery = 99% Analysis Date = 11/18/15 Pct Recovery = 99% Analysis Date = 11/13/15 Pct Recovery = 99% Analysis Date = 11/13/15 Pct Recovery = 99% Analysis Date = 11/08/15 Pct Recovery = 98% Analysis Date = 11/08/15 Pct Recovery = 98% Analysis Date = 11/03/15 Pct Recovery = 98% Analysis Date = 11/03/15 Pct Recovery = 98% Analysis Date = 10/30/15 Pct Recovery = 98% Analysis Date = 10/30/15 Pct Recovery = 98% Analysis Date = 10/25/15 Pct Recovery = 98% Analysis Date = 10/25/15 Pct Recovery = 98% Analysis Date = 10/20/15 Pct Recovery = 98% Analysis Date = 10/20/15 Pct Recovery = 98% Analysis Date = 10/15/15 Pct Recovery = 98% Analysis Date = 10/15/15 Pct Recovery = 98% Analysis Date = 10/10/15 Pct Recovery = 98% Analysis Date = 10/10/15 Pct Recovery = 98% Analysis Date = 10/06/15 Pct Recovery = 97% Analysis Date = 10/06/15 Pct Recovery = 97% Analysis Date = 10/01/15 Pct Recovery = 97% Analysis Date = 10/01/15 Pct Recovery = 97% Analysis Date = 09/26/15 Pct Recovery = 97% Analysis Date = 09/26/15 Pct Recovery = 97% Analysis Date = 09/21/15 Pct Recovery = 97% Analysis Date = 09/21/15 Pct Recovery = 97% Analysis Date = 09/16/15 Pct Recovery = 97% Analysis Date = 09/16/15 Pct Recovery = 97% Analysis Date = 09/12/15 Pct Recovery = 97% Analysis Date = 09/12/15 Pct Recovery = 97% Analysis Date = 09/07/15 Pct Recovery = 97% Analysis Date = 09/07/15 Pct Recovery = 97% Analysis Date = 09/02/15 Pct Recovery = 96% Analysis Date = 09/02/15 Pct Recovery = 96% Analysis Date = 08/28/15 Pct Recovery = 96% Analysis Date = 08/28/15 Pct Recovery = 96% Analysis Date = 08/23/15 Pct Recovery = 96% Analysis Date = 08/23/15 Pct Recovery = 96% Analysis Date = 08/19/15 Pct Recovery = 96% Analysis Date = 08/19/15 Pct Recovery = 96% Analysis Date = 08/14/15 Pct Recovery = 96% Analysis Date = 08/14/15 Pct Recovery = 96% Analysis Date = 08/09/15 Pct Recovery = 96% Analysis Date = 08/09/15 Pct Recovery = 96% Analysis Date = 08/04/15 Pct Recovery = 96% Analysis Date = 08/04/15 Pct Recovery = 96% Analysis Date = 07/30/15 Pct Recovery = 95% Analysis Date = 07/30/15 Pct Recovery = 95% Analysis Date = 07/26/15 Pct Recovery = 95% Analysis Date = 07/26/15 Pct Recovery = 95% Analysis Date = 07/21/15 Pct Recovery = 95% Analysis Date = 07/21/15 Pct Recovery = 95% Analysis Date = 07/16/15 Pct Recovery = 95% Analysis Date = 07/16/15 Pct Recovery = 95% Analysis Date = 07/11/15 Pct Recovery = 95% Analysis Date = 07/11/15 Pct Recovery = 95% Analysis Date = 07/06/15 Pct Recovery = 95% Analysis Date = 07/06/15 Pct Recovery = 95% Analysis Date = 07/02/15 Pct Recovery = 95% Analysis Date = 07/02/15 Pct Recovery = 95% Analysis Date = 06/27/15 Pct Recovery = 94% Analysis Date = 06/27/15 Pct Recovery = 94% Analysis Date = 06/22/15 Pct Recovery = 94% Analysis Date = 06/22/15 Pct Recovery = 94% Analysis Date = 06/17/15 Pct Recovery = 94% Analysis Date = 06/17/15 Pct Recovery = 94% Analysis Date = 06/12/15 Pct Recovery = 94% Analysis Date = 06/12/15 Pct Recovery = 94% Analysis Date = 06/08/15 Pct Recovery = 94% Analysis Date = 06/08/15 Pct Recovery = 94% Analysis Date = 06/03/15 Pct Recovery = 94% Analysis Date = 06/03/15 Pct Recovery = 94% Analysis Date = 05/29/15 Pct Recovery = 94% Analysis Date = 05/29/15 Pct Recovery = 94% Analysis Date = 05/24/15 Pct Recovery = 93% Analysis Date = 05/24/15 Pct Recovery = 93% Analysis Date = 05/19/15 Pct Recovery = 93% Analysis Date = 05/19/15 Pct Recovery = 93% Analysis Date = 05/15/15 Pct Recovery = 93% Analysis Date = 05/15/15 Pct Recovery = 93% Analysis Date = 05/10/15 Pct Recovery = 93% Analysis Date = 05/10/15 Pct Recovery = 93% Analysis Date = 05/05/15 Pct Recovery = 93% Analysis Date = 05/05/15 Pct Recovery = 93% Analysis Date = 04/30/15 Pct Recovery = 93% Analysis Date = 04/30/15 Pct Recovery = 93% Analysis Date = 04/25/15 Pct Recovery = 93% Analysis Date = 04/25/15 Pct Recovery = 93% Analysis Date = 04/21/15 Pct Recovery = 93% Analysis Date = 04/21/15 Pct Recovery = 93% Analysis Date = 04/16/15 Pct Recovery = 93% Analysis Date = 04/16/15 Pct Recovery = 93% Analysis Date = 04/11/15 Pct Recovery = 93% Analysis Date = 04/11/15 Pct Recovery = 93% Analysis Date = 04/06/15 Pct Recovery = 93% Analysis Date = 04/06/15 Pct Recovery = 93% Analysis Date = 04/01/15 Pct Recovery = 93% Analysis Date = 04/01/15 Pct Recovery = 93% Analysis Date = 03/28/15 Pct Recovery = 93% Analysis Date = 03/28/15 Pct Recovery = 93% Analysis Date = 03/23/15 Pct Recovery = 93% Analysis Date = 03/23/15 Pct Recovery = 93% Analysis Date = 03/18/15 Pct Recovery = 93% Analysis Date = 03/18/15 Pct Recovery = 93% Analysis Date = 03/13/15 Pct Recovery = 93% Analysis Date = 03/13/15 Pct Recovery = 93% Analysis Date = 03/08/15 Pct Recovery = 93% Analysis Date = 03/08/15 Pct Recovery = 93% Analysis Date = 03/04/15 Pct Recovery = 93% Analysis Date = 03/04/15 Pct Recovery = 93% Analysis Date = 02/27/15 Pct Recovery = 93% Analysis Date = 02/27/15 Pct Recovery = 93% Analysis Date = 02/22/15 Pct Recovery = 93% Analysis Date = 02/22/15 Pct Recovery = 93% Analysis Date = 02/17/15 Pct Recovery = 93% Analysis Date = 02/17/15 Pct Recovery = 93% Analysis Date = 02/12/15 Pct Recovery = 93% Analysis Date = 02/12/15 Pct Recovery = 93% Analysis Date = 02/08/15 Pct Recovery = 93% Analysis Date = 02/08/15 Pct Recovery = 93% Analysis Date = 02/03/15 Pct Recovery = 93% Analysis Date = 02/03/15 Pct Recovery = 93% Analysis Date = 01/29/15 Pct Recovery = 93% Analysis Date = 01/29/15 Pct Recovery = 93% Analysis Date = 01/24/15 Pct Recovery = 93% Analysis Date = 01/24/15 Pct Recovery = 93% Analysis Date = 01/19/15 Pct Recovery = 93% Analysis Date = 01/19/15 Pct Recovery = 93% Analysis Date = 01/15/15 Pct Recovery = 93% Analysis Date = 01/15/15 Pct Recovery = 93% Analysis Date = 01/10/15 Pct Recovery = 93% Analysis Date = 01/10/15 Pct Recovery = 93% Analysis Date = 01/05/15 Pct Recovery = 93% Analysis Date = 01/05/15 Pct Recovery = 93% Analysis Date = 12/31/14 Pct Recovery = 93% Analysis Date = 12/31/14 Pct Recovery = 93% Analysis Date = 12/26/14 Pct Recovery = 93% Analysis Date = 12/26/14 Pct Recovery = 93% Analysis Date = 12/22/14 Pct Recovery = 92% Analysis Date = 12/22/14 Pct Recovery = 92% Analysis Date = 12/17/14 Pct Recovery = 92% Analysis Date = 12/17/14 Pct Recovery = 92% Analysis Date = 12/12/14 Pct Recovery = 92% Analysis Date = 12/12/14 Pct Recovery = 92% Analysis Date = 12/07/14 Pct Recovery = 92% Analysis Date = 12/07/14 Pct Recovery = 92% Analysis Date = 12/02/14 Pct Recovery = 92% Analysis Date = 12/02/14 Pct Recovery = 92% Analysis Date = 11/28/14 Pct Recovery = 92% Analysis Date = 11/28/14 Pct Recovery = 92% Analysis Date = 11/23/14 Pct Recovery = 92% Analysis Date = 11/23/14 Pct Recovery = 92% Analysis Date = 11/18/14 Pct Recovery = 92% Analysis Date = 11/18/14 Pct Recovery = 92% Analysis Date = 11/13/14 Pct Recovery = 92% Analysis Date = 11/13/14 Pct Recovery = 92% Analysis Date = 11/08/14 Pct Recovery = 92% Analysis Date = 11/08/14 Pct Recovery = 92% Analysis Date = 11/04/14 Pct Recovery = 92% Analysis Date = 11/04/14 Pct Recovery = 92% Analysis Date = 10/30/14 Pct Recovery = 92% Analysis Date = 10/30/14 Pct Recovery = 92% Analysis Date = 10/25/14 Pct Recovery = 92% Analysis Date = 10/25/14 Pct Recovery = 92% Analysis Date = 10/20/14 Pct Recovery = 92% Analysis Date = 10/20/14 Pct Recovery = 92% Analysis Date = 10/15/14 Pct Recovery = 92% Analysis Date = 10/15/14 Pct Recovery = 92% Analysis Date = 10/11/14 Pct Recovery = 92% Analysis Date = 10/11/14 Pct Recovery = 92% Analysis Date = 10/06/14 Pct Recovery = 92% Analysis Date = 10/06/14 Pct Recovery = 92% Analysis Date = 10/01/14 Pct Recovery = 92% Analysis Date = 10/01/14 Pct Recovery = 92% Analysis Date = 09/26/14 Pct Recovery = 92% Analysis Date = 09/26/14 Pct Recovery = 92% Analysis Date = 09/21/14 Pct Recovery = 92% Analysis Date = 09/21/14 Pct Recovery = 92% Analysis Date = 09/17/14 Pct Recovery = 92% Analysis Date = 09/17/14 Pct Recovery = 92% Analysis Date = 09/12/14 Pct Recovery = 92% Analysis Date = 09/12/14 Pct Recovery = 92% Analysis Date = 09/07/14 Pct Recovery = 92% Analysis Date = 09/07/14 Pct Recovery = 92% Analysis Date = 09/02/14 Pct Recovery = 92% Analysis Date = 09/02/14 Pct Recovery = 92% Analysis Date = 08/28/14 Pct Recovery = 92% Analysis Date = 08/28/14 Pct Recovery = 92% Analysis Date = 08/24/14 Pct Recovery = 92% Analysis Date = 08/24/14 Pct Recovery = 92% Analysis Date = 08/19/14 Pct Recovery = 92% Analysis Date = 08/19/14 Pct Recovery = 92% Analysis Date = 08/14/14 Pct Recovery = 92% Analysis Date = 08/14/14 Pct Recovery = 92% Analysis Date = 08/09/14 Pct Recovery = 92% Analysis Date = 08/09/14 Pct Recovery = 92% Analysis Date = 08/04/14 Pct Recovery = 92% Analysis Date = 08/04/14 Pct Recovery = 92% Analysis Date = 07/31/14 Pct Recovery = 92% Analysis Date = 07/31/14 Pct Recovery = 92% Analysis Date = 07/26/14 Pct Recovery = 92% Analysis Date = 07/26/14 Pct Recovery = 92% Analysis Date = 07/21/14 Pct Recovery = 92% Analysis Date = 07/21/14 Pct Recovery = 92% Analysis Date = 07/16/14 Pct Recovery = 92% Analysis Date = 07/16/14 Pct Recovery = 92% Analysis Date = 07/11/14 Pct Recovery = 92% Analysis Date = 07/11/14 Pct Recovery = 92% Analysis Date = 07/07/14 Pct Recovery = 92% Analysis Date = 07/07/14 Pct Recovery = 92% Analysis Date = 07/02/14 Pct Recovery = 92% Analysis Date = 07/02/14 Pct Recovery = 92% Analysis Date = 06/27/14 Pct Recovery = 92% Analysis Date = 06/27/14 Pct Recovery = 92% Analysis Date = 06/22/14 Pct Recovery = 92% Analysis Date = 06/22/14 Pct Recovery = 92% Analysis Date = 06/17/14 Pct Recovery = 92% Analysis Date = 06/17/14 Pct Recovery = 92% Analysis Date = 06/13/14 Pct Recovery = 92% Analysis Date = 06/13/14 Pct Recovery = 92% Analysis Date = 06/08/14 Pct Recovery = 92% Analysis Date = 06/08/14 Pct Recovery = 92% Analysis Date = 06/03/14 Pct Recovery = 92% Analysis Date = 06/03/14 Pct Recovery = 92% Analysis Date = 05/29/14 Pct Recovery = 92% Analysis Date = 05/29/14 Pct Recovery = 92% Analysis Date = 05/24/14 Pct Recovery = 92% Analysis Date = 05/24/14 Pct Recovery = 92% Analysis Date = 05/20/14 Pct Recovery = 92% Analysis Date = 05/20/14 Pct Recovery = 92% Analysis Date = 05/15/14 Pct Recovery = 92% Analysis Date = 05/15/14 Pct Recovery = 92% Analysis Date = 05/10/14 Pct Recovery = 92% Analysis Date = 05/10/14 Pct Recovery = 92% Analysis Date = 05/05/14 Pct Recovery = 92% Analysis Date = 05/05/14 Pct Recovery = 92% Analysis Date = 05/01/14 Pct Recovery = 92% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
TETRAHYDROFURAN

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 50 98% 11% 100% 13%
Total 50 98% 11% 100% 13%

Sample Statistics
TETRAHYDROFURAN

Characteristic N % % Basis
Plotted 50 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 50 .  
False Negatives 0 0% 0 out of 50
Not Spiked 23 .  
False Positives 0 0% 0 out of 23

BQS OBSP Determination:
TOLUENE
METHOD: 4440 , TESTIDCODE: 34010GCM66
Open Data Set

Analysis Date = 05/13/16 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 567% Analysis Date = 12/16/16 SpikeMix = NSI 041816AVOC: 40 µl & ChemService 5082900: 40 µl Pct Recovery = 132% Analysis Date = 08/04/16 SpikeMix = Crescent 03FF058: 40 µl & Supelco LC20141V: 40 µl Pct Recovery = 126% Analysis Date = 07/20/16 SpikeMix = Supelco LC20141V: 40 µl & Accu 216041125: 40 µl Pct Recovery = 89% Analysis Date = 08/26/16 SpikeMix = NSI 041816AVOC: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 118% Analysis Date = 08/12/16 SpikeMix = ChemService 5082900: 25 µl & Phenova B20160319: 25 µl Pct Recovery = 94% Analysis Date = 06/30/16 SpikeMix = Crescent 03FF058: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 118% Analysis Date = 11/21/16 SpikeMix = Crescent 03FF058: 25 µl & Supelco LC20141V: 25 µl Pct Recovery = 118% Analysis Date = 09/08/16 SpikeMix = Supelco LC20141V: 25 µl & Accu 216041125: 25 µl Pct Recovery = 95% Analysis Date = 03/19/15 SpikeMix = Spex Organics C1140417015: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 100% Analysis Date = 11/22/14 SpikeMix = NSI 032614: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 100% Analysis Date = 08/19/14 SpikeMix = Spex Organics C1140417015: 20 µl & Accu 214031115: 20 µl Pct Recovery = 100% Analysis Date = 08/16/14 SpikeMix = ERA 0227-14-06.1A: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 100% Analysis Date = 08/15/15 SpikeMix = Supelco LC13545: 25 µl & Crescent 04EE008: 25 µl Pct Recovery = 107% Analysis Date = 06/16/15 SpikeMix = ERA 0406-15-03: 25 µl & Supelco LC13545: 25 µl Pct Recovery = 93% Analysis Date = 11/29/16 SpikeMix = ChemService 5082900: 15 µl & Phenova B20160319: 15 µl Pct Recovery = 98% Analysis Date = 09/28/16 SpikeMix = Crescent 03FF058: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 137% Analysis Date = 06/30/16 SpikeMix = ChemService 5082900: 15 µl & Accu 216041125: 15 µl Pct Recovery = 98% Analysis Date = 06/10/16 SpikeMix = NSI 041816AVOC: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 137% Analysis Date = 10/13/16 SpikeMix = NSI 041816AVOC: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 118% Analysis Date = 05/27/16 SpikeMix = Phenova B20160319: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 99% Analysis Date = 04/26/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 108% Analysis Date = 02/05/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 87% Analysis Date = 11/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 87% Analysis Date = 10/16/15 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 108% Analysis Date = 05/09/15 SpikeMix = Spex Organics EN150428007: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 108% Analysis Date = 04/02/16 SpikeMix = Supelco LC13545: 15 µl & Accu 215041380: 15 µl Pct Recovery = 111% Analysis Date = 12/18/15 SpikeMix = Supelco LC13545: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 111% Analysis Date = 11/06/14 SpikeMix = Spex Organics C1140417015: 10 µl & Crescent 03DD004: 10 µl Pct Recovery = 100% Analysis Date = 09/09/14 SpikeMix = NSI 032614: 10 µl & Spex Organics C1140417015: 10 µl Pct Recovery = 125% Analysis Date = 07/23/14 SpikeMix = Spex Organics C1140417015: 10 µl & Accu 214031115: 10 µl Pct Recovery = 100% Analysis Date = 07/11/14 SpikeMix = Spex Organics C1140417015: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 100% Analysis Date = 02/18/16 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 97% Analysis Date = 11/12/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 130% Analysis Date = 09/03/15 SpikeMix = NSI 050515AVOC: 10 µl & Spex Organics EN150428007: 10 µl Pct Recovery = 97% Analysis Date = 05/21/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 130% Analysis Date = 03/17/16 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 100% Analysis Date = 12/10/15 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 100% Analysis Date = 06/27/15 SpikeMix = ERA 0406-15-03: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 100% Analysis Date = 05/09/15 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 100% Analysis Date = 12/15/16 Pct Recovery = 104% Analysis Date = 12/11/16 Pct Recovery = 105% Analysis Date = 12/11/16 Pct Recovery = 105% Analysis Date = 12/07/16 Pct Recovery = 106% Analysis Date = 12/07/16 Pct Recovery = 106% Analysis Date = 12/02/16 Pct Recovery = 107% Analysis Date = 12/02/16 Pct Recovery = 107% Analysis Date = 11/28/16 Pct Recovery = 108% Analysis Date = 11/28/16 Pct Recovery = 108% Analysis Date = 11/23/16 Pct Recovery = 109% Analysis Date = 11/23/16 Pct Recovery = 109% Analysis Date = 11/19/16 Pct Recovery = 110% Analysis Date = 11/19/16 Pct Recovery = 110% Analysis Date = 11/14/16 Pct Recovery = 111% Analysis Date = 11/14/16 Pct Recovery = 111% Analysis Date = 11/10/16 Pct Recovery = 112% Analysis Date = 11/10/16 Pct Recovery = 112% Analysis Date = 11/05/16 Pct Recovery = 113% Analysis Date = 11/05/16 Pct Recovery = 113% Analysis Date = 11/01/16 Pct Recovery = 114% Analysis Date = 11/01/16 Pct Recovery = 114% Analysis Date = 10/28/16 Pct Recovery = 115% Analysis Date = 10/28/16 Pct Recovery = 115% Analysis Date = 10/23/16 Pct Recovery = 116% Analysis Date = 10/23/16 Pct Recovery = 116% Analysis Date = 10/19/16 Pct Recovery = 117% Analysis Date = 10/19/16 Pct Recovery = 117% Analysis Date = 10/14/16 Pct Recovery = 118% Analysis Date = 10/14/16 Pct Recovery = 118% Analysis Date = 10/10/16 Pct Recovery = 119% Analysis Date = 10/10/16 Pct Recovery = 119% Analysis Date = 10/05/16 Pct Recovery = 119% Analysis Date = 10/05/16 Pct Recovery = 119% Analysis Date = 10/01/16 Pct Recovery = 120% Analysis Date = 10/01/16 Pct Recovery = 120% Analysis Date = 09/26/16 Pct Recovery = 121% Analysis Date = 09/26/16 Pct Recovery = 121% Analysis Date = 09/22/16 Pct Recovery = 122% Analysis Date = 09/22/16 Pct Recovery = 122% Analysis Date = 09/18/16 Pct Recovery = 123% Analysis Date = 09/18/16 Pct Recovery = 123% Analysis Date = 09/13/16 Pct Recovery = 124% Analysis Date = 09/13/16 Pct Recovery = 124% Analysis Date = 09/09/16 Pct Recovery = 125% Analysis Date = 09/09/16 Pct Recovery = 125% Analysis Date = 09/04/16 Pct Recovery = 126% Analysis Date = 09/04/16 Pct Recovery = 126% Analysis Date = 08/31/16 Pct Recovery = 127% Analysis Date = 08/31/16 Pct Recovery = 127% Analysis Date = 08/26/16 Pct Recovery = 128% Analysis Date = 08/26/16 Pct Recovery = 128% Analysis Date = 08/22/16 Pct Recovery = 129% Analysis Date = 08/22/16 Pct Recovery = 129% Analysis Date = 08/17/16 Pct Recovery = 129% Analysis Date = 08/17/16 Pct Recovery = 129% Analysis Date = 08/13/16 Pct Recovery = 130% Analysis Date = 08/13/16 Pct Recovery = 130% Analysis Date = 08/09/16 Pct Recovery = 131% Analysis Date = 08/09/16 Pct Recovery = 131% Analysis Date = 08/04/16 Pct Recovery = 132% Analysis Date = 08/04/16 Pct Recovery = 132% Analysis Date = 07/31/16 Pct Recovery = 132% Analysis Date = 07/31/16 Pct Recovery = 132% Analysis Date = 07/26/16 Pct Recovery = 133% Analysis Date = 07/26/16 Pct Recovery = 133% Analysis Date = 07/22/16 Pct Recovery = 134% Analysis Date = 07/22/16 Pct Recovery = 134% Analysis Date = 07/17/16 Pct Recovery = 135% Analysis Date = 07/17/16 Pct Recovery = 135% Analysis Date = 07/13/16 Pct Recovery = 135% Analysis Date = 07/13/16 Pct Recovery = 135% Analysis Date = 07/08/16 Pct Recovery = 136% Analysis Date = 07/08/16 Pct Recovery = 136% Analysis Date = 07/04/16 Pct Recovery = 137% Analysis Date = 07/04/16 Pct Recovery = 137% Analysis Date = 06/30/16 Pct Recovery = 137% Analysis Date = 06/30/16 Pct Recovery = 137% Analysis Date = 06/25/16 Pct Recovery = 138% Analysis Date = 06/25/16 Pct Recovery = 138% Analysis Date = 06/21/16 Pct Recovery = 138% Analysis Date = 06/21/16 Pct Recovery = 138% Analysis Date = 06/16/16 Pct Recovery = 139% Analysis Date = 06/16/16 Pct Recovery = 139% Analysis Date = 06/12/16 Pct Recovery = 140% Analysis Date = 06/12/16 Pct Recovery = 140% Analysis Date = 06/07/16 Pct Recovery = 140% Analysis Date = 06/07/16 Pct Recovery = 140% Analysis Date = 06/03/16 Pct Recovery = 140% Analysis Date = 06/03/16 Pct Recovery = 140% Analysis Date = 05/29/16 Pct Recovery = 139% Analysis Date = 05/29/16 Pct Recovery = 139% Analysis Date = 05/25/16 Pct Recovery = 139% Analysis Date = 05/25/16 Pct Recovery = 139% Analysis Date = 05/21/16 Pct Recovery = 139% Analysis Date = 05/21/16 Pct Recovery = 139% Analysis Date = 05/16/16 Pct Recovery = 139% Analysis Date = 05/16/16 Pct Recovery = 139% Analysis Date = 05/12/16 Pct Recovery = 139% Analysis Date = 05/12/16 Pct Recovery = 139% Analysis Date = 05/07/16 Pct Recovery = 138% Analysis Date = 05/07/16 Pct Recovery = 138% Analysis Date = 05/03/16 Pct Recovery = 138% Analysis Date = 05/03/16 Pct Recovery = 138% Analysis Date = 04/28/16 Pct Recovery = 138% Analysis Date = 04/28/16 Pct Recovery = 138% Analysis Date = 04/24/16 Pct Recovery = 138% Analysis Date = 04/24/16 Pct Recovery = 138% Analysis Date = 04/19/16 Pct Recovery = 137% Analysis Date = 04/19/16 Pct Recovery = 137% Analysis Date = 04/15/16 Pct Recovery = 137% Analysis Date = 04/15/16 Pct Recovery = 137% Analysis Date = 04/11/16 Pct Recovery = 137% Analysis Date = 04/11/16 Pct Recovery = 137% Analysis Date = 04/06/16 Pct Recovery = 136% Analysis Date = 04/06/16 Pct Recovery = 136% Analysis Date = 04/02/16 Pct Recovery = 136% Analysis Date = 04/02/16 Pct Recovery = 136% Analysis Date = 03/28/16 Pct Recovery = 136% Analysis Date = 03/28/16 Pct Recovery = 136% Analysis Date = 03/24/16 Pct Recovery = 136% Analysis Date = 03/24/16 Pct Recovery = 136% Analysis Date = 03/19/16 Pct Recovery = 135% Analysis Date = 03/19/16 Pct Recovery = 135% Analysis Date = 03/15/16 Pct Recovery = 135% Analysis Date = 03/15/16 Pct Recovery = 135% Analysis Date = 03/10/16 Pct Recovery = 134% Analysis Date = 03/10/16 Pct Recovery = 134% Analysis Date = 03/06/16 Pct Recovery = 133% Analysis Date = 03/06/16 Pct Recovery = 133% Analysis Date = 03/02/16 Pct Recovery = 132% Analysis Date = 03/02/16 Pct Recovery = 132% Analysis Date = 02/26/16 Pct Recovery = 131% Analysis Date = 02/26/16 Pct Recovery = 131% Analysis Date = 02/22/16 Pct Recovery = 130% Analysis Date = 02/22/16 Pct Recovery = 130% Analysis Date = 02/17/16 Pct Recovery = 129% Analysis Date = 02/17/16 Pct Recovery = 129% Analysis Date = 02/13/16 Pct Recovery = 128% Analysis Date = 02/13/16 Pct Recovery = 128% Analysis Date = 02/08/16 Pct Recovery = 127% Analysis Date = 02/08/16 Pct Recovery = 127% Analysis Date = 02/04/16 Pct Recovery = 126% Analysis Date = 02/04/16 Pct Recovery = 126% Analysis Date = 01/30/16 Pct Recovery = 125% Analysis Date = 01/30/16 Pct Recovery = 125% Analysis Date = 01/26/16 Pct Recovery = 125% Analysis Date = 01/26/16 Pct Recovery = 125% Analysis Date = 01/22/16 Pct Recovery = 124% Analysis Date = 01/22/16 Pct Recovery = 124% Analysis Date = 01/17/16 Pct Recovery = 123% Analysis Date = 01/17/16 Pct Recovery = 123% Analysis Date = 01/13/16 Pct Recovery = 122% Analysis Date = 01/13/16 Pct Recovery = 122% Analysis Date = 01/08/16 Pct Recovery = 121% Analysis Date = 01/08/16 Pct Recovery = 121% Analysis Date = 01/04/16 Pct Recovery = 120% Analysis Date = 01/04/16 Pct Recovery = 120% Analysis Date = 12/30/15 Pct Recovery = 119% Analysis Date = 12/30/15 Pct Recovery = 119% Analysis Date = 12/26/15 Pct Recovery = 118% Analysis Date = 12/26/15 Pct Recovery = 118% Analysis Date = 12/21/15 Pct Recovery = 117% Analysis Date = 12/21/15 Pct Recovery = 117% Analysis Date = 12/17/15 Pct Recovery = 116% Analysis Date = 12/17/15 Pct Recovery = 116% Analysis Date = 12/13/15 Pct Recovery = 116% Analysis Date = 12/13/15 Pct Recovery = 116% Analysis Date = 12/08/15 Pct Recovery = 115% Analysis Date = 12/08/15 Pct Recovery = 115% Analysis Date = 12/04/15 Pct Recovery = 114% Analysis Date = 12/04/15 Pct Recovery = 114% Analysis Date = 11/29/15 Pct Recovery = 114% Analysis Date = 11/29/15 Pct Recovery = 114% Analysis Date = 11/25/15 Pct Recovery = 113% Analysis Date = 11/25/15 Pct Recovery = 113% Analysis Date = 11/20/15 Pct Recovery = 113% Analysis Date = 11/20/15 Pct Recovery = 113% Analysis Date = 11/16/15 Pct Recovery = 112% Analysis Date = 11/16/15 Pct Recovery = 112% Analysis Date = 11/11/15 Pct Recovery = 111% Analysis Date = 11/11/15 Pct Recovery = 111% Analysis Date = 11/07/15 Pct Recovery = 111% Analysis Date = 11/07/15 Pct Recovery = 111% Analysis Date = 11/03/15 Pct Recovery = 111% Analysis Date = 11/03/15 Pct Recovery = 111% Analysis Date = 10/29/15 Pct Recovery = 110% Analysis Date = 10/29/15 Pct Recovery = 110% Analysis Date = 10/25/15 Pct Recovery = 110% Analysis Date = 10/25/15 Pct Recovery = 110% Analysis Date = 10/20/15 Pct Recovery = 110% Analysis Date = 10/20/15 Pct Recovery = 110% Analysis Date = 10/16/15 Pct Recovery = 109% Analysis Date = 10/16/15 Pct Recovery = 109% Analysis Date = 10/11/15 Pct Recovery = 109% Analysis Date = 10/11/15 Pct Recovery = 109% Analysis Date = 10/07/15 Pct Recovery = 109% Analysis Date = 10/07/15 Pct Recovery = 109% Analysis Date = 10/02/15 Pct Recovery = 108% Analysis Date = 10/02/15 Pct Recovery = 108% Analysis Date = 09/28/15 Pct Recovery = 108% Analysis Date = 09/28/15 Pct Recovery = 108% Analysis Date = 09/24/15 Pct Recovery = 108% Analysis Date = 09/24/15 Pct Recovery = 108% Analysis Date = 09/19/15 Pct Recovery = 107% Analysis Date = 09/19/15 Pct Recovery = 107% Analysis Date = 09/15/15 Pct Recovery = 107% Analysis Date = 09/15/15 Pct Recovery = 107% Analysis Date = 09/10/15 Pct Recovery = 107% Analysis Date = 09/10/15 Pct Recovery = 107% Analysis Date = 09/06/15 Pct Recovery = 106% Analysis Date = 09/06/15 Pct Recovery = 106% Analysis Date = 09/01/15 Pct Recovery = 106% Analysis Date = 09/01/15 Pct Recovery = 106% Analysis Date = 08/28/15 Pct Recovery = 106% Analysis Date = 08/28/15 Pct Recovery = 106% Analysis Date = 08/23/15 Pct Recovery = 106% Analysis Date = 08/23/15 Pct Recovery = 106% Analysis Date = 08/19/15 Pct Recovery = 106% Analysis Date = 08/19/15 Pct Recovery = 106% Analysis Date = 08/15/15 Pct Recovery = 106% Analysis Date = 08/15/15 Pct Recovery = 106% Analysis Date = 08/10/15 Pct Recovery = 106% Analysis Date = 08/10/15 Pct Recovery = 106% Analysis Date = 08/06/15 Pct Recovery = 105% Analysis Date = 08/06/15 Pct Recovery = 105% Analysis Date = 08/01/15 Pct Recovery = 105% Analysis Date = 08/01/15 Pct Recovery = 105% Analysis Date = 07/28/15 Pct Recovery = 105% Analysis Date = 07/28/15 Pct Recovery = 105% Analysis Date = 07/23/15 Pct Recovery = 105% Analysis Date = 07/23/15 Pct Recovery = 105% Analysis Date = 07/19/15 Pct Recovery = 105% Analysis Date = 07/19/15 Pct Recovery = 105% Analysis Date = 07/14/15 Pct Recovery = 105% Analysis Date = 07/14/15 Pct Recovery = 105% Analysis Date = 07/10/15 Pct Recovery = 105% Analysis Date = 07/10/15 Pct Recovery = 105% Analysis Date = 07/06/15 Pct Recovery = 105% Analysis Date = 07/06/15 Pct Recovery = 105% Analysis Date = 07/01/15 Pct Recovery = 105% Analysis Date = 07/01/15 Pct Recovery = 105% Analysis Date = 06/27/15 Pct Recovery = 105% Analysis Date = 06/27/15 Pct Recovery = 105% Analysis Date = 06/22/15 Pct Recovery = 105% Analysis Date = 06/22/15 Pct Recovery = 105% Analysis Date = 06/18/15 Pct Recovery = 105% Analysis Date = 06/18/15 Pct Recovery = 105% Analysis Date = 06/13/15 Pct Recovery = 105% Analysis Date = 06/13/15 Pct Recovery = 105% Analysis Date = 06/09/15 Pct Recovery = 105% Analysis Date = 06/09/15 Pct Recovery = 105% Analysis Date = 06/04/15 Pct Recovery = 105% Analysis Date = 06/04/15 Pct Recovery = 105% Analysis Date = 05/31/15 Pct Recovery = 105% Analysis Date = 05/31/15 Pct Recovery = 105% Analysis Date = 05/27/15 Pct Recovery = 105% Analysis Date = 05/27/15 Pct Recovery = 105% Analysis Date = 05/22/15 Pct Recovery = 105% Analysis Date = 05/22/15 Pct Recovery = 105% Analysis Date = 05/18/15 Pct Recovery = 105% Analysis Date = 05/18/15 Pct Recovery = 105% Analysis Date = 05/13/15 Pct Recovery = 105% Analysis Date = 05/13/15 Pct Recovery = 105% Analysis Date = 05/09/15 Pct Recovery = 105% Analysis Date = 05/09/15 Pct Recovery = 105% Analysis Date = 05/04/15 Pct Recovery = 105% Analysis Date = 05/04/15 Pct Recovery = 105% Analysis Date = 04/30/15 Pct Recovery = 105% Analysis Date = 04/30/15 Pct Recovery = 105% Analysis Date = 04/25/15 Pct Recovery = 105% Analysis Date = 04/25/15 Pct Recovery = 105% Analysis Date = 04/21/15 Pct Recovery = 105% Analysis Date = 04/21/15 Pct Recovery = 105% Analysis Date = 04/17/15 Pct Recovery = 105% Analysis Date = 04/17/15 Pct Recovery = 105% Analysis Date = 04/12/15 Pct Recovery = 105% Analysis Date = 04/12/15 Pct Recovery = 105% Analysis Date = 04/08/15 Pct Recovery = 105% Analysis Date = 04/08/15 Pct Recovery = 105% Analysis Date = 04/03/15 Pct Recovery = 105% Analysis Date = 04/03/15 Pct Recovery = 105% Analysis Date = 03/30/15 Pct Recovery = 105% Analysis Date = 03/30/15 Pct Recovery = 105% Analysis Date = 03/25/15 Pct Recovery = 105% Analysis Date = 03/25/15 Pct Recovery = 105% Analysis Date = 03/21/15 Pct Recovery = 105% Analysis Date = 03/21/15 Pct Recovery = 105% Analysis Date = 03/16/15 Pct Recovery = 105% Analysis Date = 03/16/15 Pct Recovery = 105% Analysis Date = 03/12/15 Pct Recovery = 105% Analysis Date = 03/12/15 Pct Recovery = 105% Analysis Date = 03/08/15 Pct Recovery = 105% Analysis Date = 03/08/15 Pct Recovery = 105% Analysis Date = 03/03/15 Pct Recovery = 105% Analysis Date = 03/03/15 Pct Recovery = 105% Analysis Date = 02/27/15 Pct Recovery = 105% Analysis Date = 02/27/15 Pct Recovery = 105% Analysis Date = 02/22/15 Pct Recovery = 104% Analysis Date = 02/22/15 Pct Recovery = 104% Analysis Date = 02/18/15 Pct Recovery = 104% Analysis Date = 02/18/15 Pct Recovery = 104% Analysis Date = 02/13/15 Pct Recovery = 104% Analysis Date = 02/13/15 Pct Recovery = 104% Analysis Date = 02/09/15 Pct Recovery = 104% Analysis Date = 02/09/15 Pct Recovery = 104% Analysis Date = 02/04/15 Pct Recovery = 104% Analysis Date = 02/04/15 Pct Recovery = 104% Analysis Date = 01/31/15 Pct Recovery = 104% Analysis Date = 01/31/15 Pct Recovery = 104% Analysis Date = 01/27/15 Pct Recovery = 104% Analysis Date = 01/27/15 Pct Recovery = 104% Analysis Date = 01/22/15 Pct Recovery = 104% Analysis Date = 01/22/15 Pct Recovery = 104% Analysis Date = 01/18/15 Pct Recovery = 104% Analysis Date = 01/18/15 Pct Recovery = 104% Analysis Date = 01/13/15 Pct Recovery = 104% Analysis Date = 01/13/15 Pct Recovery = 104% Analysis Date = 01/09/15 Pct Recovery = 104% Analysis Date = 01/09/15 Pct Recovery = 104% Analysis Date = 01/04/15 Pct Recovery = 104% Analysis Date = 01/04/15 Pct Recovery = 104% Analysis Date = 12/31/14 Pct Recovery = 104% Analysis Date = 12/31/14 Pct Recovery = 104% Analysis Date = 12/26/14 Pct Recovery = 104% Analysis Date = 12/26/14 Pct Recovery = 104% Analysis Date = 12/22/14 Pct Recovery = 104% Analysis Date = 12/22/14 Pct Recovery = 104% Analysis Date = 12/18/14 Pct Recovery = 104% Analysis Date = 12/18/14 Pct Recovery = 104% Analysis Date = 12/13/14 Pct Recovery = 104% Analysis Date = 12/13/14 Pct Recovery = 104% Analysis Date = 12/09/14 Pct Recovery = 104% Analysis Date = 12/09/14 Pct Recovery = 104% Analysis Date = 12/04/14 Pct Recovery = 104% Analysis Date = 12/04/14 Pct Recovery = 104% Analysis Date = 11/30/14 Pct Recovery = 104% Analysis Date = 11/30/14 Pct Recovery = 104% Analysis Date = 11/25/14 Pct Recovery = 104% Analysis Date = 11/25/14 Pct Recovery = 104% Analysis Date = 11/21/14 Pct Recovery = 104% Analysis Date = 11/21/14 Pct Recovery = 104% Analysis Date = 11/16/14 Pct Recovery = 104% Analysis Date = 11/16/14 Pct Recovery = 104% Analysis Date = 11/12/14 Pct Recovery = 104% Analysis Date = 11/12/14 Pct Recovery = 104% Analysis Date = 11/08/14 Pct Recovery = 104% Analysis Date = 11/08/14 Pct Recovery = 104% Analysis Date = 11/03/14 Pct Recovery = 104% Analysis Date = 11/03/14 Pct Recovery = 104% Analysis Date = 10/30/14 Pct Recovery = 104% Analysis Date = 10/30/14 Pct Recovery = 104% Analysis Date = 10/25/14 Pct Recovery = 104% Analysis Date = 10/25/14 Pct Recovery = 104% Analysis Date = 10/21/14 Pct Recovery = 104% Analysis Date = 10/21/14 Pct Recovery = 104% Analysis Date = 10/16/14 Pct Recovery = 104% Analysis Date = 10/16/14 Pct Recovery = 104% Analysis Date = 10/12/14 Pct Recovery = 104% Analysis Date = 10/12/14 Pct Recovery = 104% Analysis Date = 10/07/14 Pct Recovery = 104% Analysis Date = 10/07/14 Pct Recovery = 104% Analysis Date = 10/03/14 Pct Recovery = 104% Analysis Date = 10/03/14 Pct Recovery = 104% Analysis Date = 09/29/14 Pct Recovery = 104% Analysis Date = 09/29/14 Pct Recovery = 104% Analysis Date = 09/24/14 Pct Recovery = 104% Analysis Date = 09/24/14 Pct Recovery = 104% Analysis Date = 09/20/14 Pct Recovery = 104% Analysis Date = 09/20/14 Pct Recovery = 104% Analysis Date = 09/15/14 Pct Recovery = 104% Analysis Date = 09/15/14 Pct Recovery = 104% Analysis Date = 09/11/14 Pct Recovery = 104% Analysis Date = 09/11/14 Pct Recovery = 104% Analysis Date = 09/06/14 Pct Recovery = 104% Analysis Date = 09/06/14 Pct Recovery = 104% Analysis Date = 09/02/14 Pct Recovery = 104% Analysis Date = 09/02/14 Pct Recovery = 104% Analysis Date = 08/28/14 Pct Recovery = 104% Analysis Date = 08/28/14 Pct Recovery = 104% Analysis Date = 08/24/14 Pct Recovery = 104% Analysis Date = 08/24/14 Pct Recovery = 104% Analysis Date = 08/20/14 Pct Recovery = 104% Analysis Date = 08/20/14 Pct Recovery = 104% Analysis Date = 08/15/14 Pct Recovery = 104% Analysis Date = 08/15/14 Pct Recovery = 104% Analysis Date = 08/11/14 Pct Recovery = 104% Analysis Date = 08/11/14 Pct Recovery = 104% Analysis Date = 08/06/14 Pct Recovery = 104% Analysis Date = 08/06/14 Pct Recovery = 104% Analysis Date = 08/02/14 Pct Recovery = 104% Analysis Date = 08/02/14 Pct Recovery = 104% Analysis Date = 07/28/14 Pct Recovery = 104% Analysis Date = 07/28/14 Pct Recovery = 104% Analysis Date = 07/24/14 Pct Recovery = 104% Analysis Date = 07/24/14 Pct Recovery = 104% Analysis Date = 07/19/14 Pct Recovery = 103% Analysis Date = 07/19/14 Pct Recovery = 103% Analysis Date = 07/15/14 Pct Recovery = 103% Analysis Date = 07/15/14 Pct Recovery = 103% Analysis Date = 07/11/14 Pct Recovery = 103% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
TOLUENE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 40 119% 74% 100% 15%
Total 40 119% 74% 100% 15%

Sample Statistics
TOLUENE

Characteristic N % % Basis
Plotted 40 100% Spiked
Estimated Values 2 5% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 40 .  
False Negatives 0 0% 0 out of 40
Not Spiked 25 .  
False Positives 3 12% 3 out of 25

BQS OBSP Determination:
TRANS-1,2-DICHLOROETHYLENE
METHOD: 4440 , TESTIDCODE: 34546GCM66
Open Data Set

Analysis Date = 08/04/16 SpikeMix = Crescent 03FF058: 40 µl & Supelco LC20141V: 40 µl Pct Recovery = 108% Analysis Date = 07/20/16 SpikeMix = Supelco LC20141V: 40 µl & Accu 216041125: 40 µl Pct Recovery = 107% Analysis Date = 04/09/15 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 88% Analysis Date = 03/06/15 SpikeMix = ERA 0227-14-06.1A: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 95% Analysis Date = 11/14/14 SpikeMix = Crescent 03DD004: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 92% Analysis Date = 08/16/14 SpikeMix = ERA 0227-14-06.1A: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 96% Analysis Date = 07/01/14 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 103% Analysis Date = 11/21/16 SpikeMix = Crescent 03FF058: 25 µl & Supelco LC20141V: 25 µl Pct Recovery = 105% Analysis Date = 09/08/16 SpikeMix = Supelco LC20141V: 25 µl & Accu 216041125: 25 µl Pct Recovery = 110% Analysis Date = 11/22/14 SpikeMix = NSI 032614: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 98% Analysis Date = 06/10/14 SpikeMix = Crescent 03DD004: 20 µl & NSI 032614: 20 µl Pct Recovery = 101% Analysis Date = 06/10/14 SpikeMix = NSI 032614: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 112% Analysis Date = 05/01/14 SpikeMix = Accu 214031115: 20 µl & NSI 032614: 20 µl Pct Recovery = 95% Analysis Date = 07/13/15 SpikeMix = Crescent 04EE008: 25 µl & NSI 050515AVOC: 25 µl Pct Recovery = 107% Analysis Date = 09/29/15 SpikeMix = Accu 215041380: 25 µl & ERA 0406-15-03: 25 µl Pct Recovery = 110% Analysis Date = 06/16/15 SpikeMix = ERA 0406-15-03: 25 µl & Supelco LC13545: 25 µl Pct Recovery = 103% Analysis Date = 10/13/16 SpikeMix = NSI 041816AVOC: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 174% Analysis Date = 05/27/16 SpikeMix = Phenova B20160319: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 105% Analysis Date = 11/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 99% Analysis Date = 10/17/15 SpikeMix = Crescent 04EE008: 15 µl & NSI 050515AVOC: 15 µl Pct Recovery = 96% Analysis Date = 06/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Accu 215041380: 15 µl Pct Recovery = 104% Analysis Date = 04/26/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 104% Analysis Date = 03/04/16 SpikeMix = Accu 215041380: 15 µl & ERA 0406-15-03: 15 µl Pct Recovery = 104% Analysis Date = 02/05/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 101% Analysis Date = 10/16/15 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 101% Analysis Date = 01/13/15 SpikeMix = Accu 214031115: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 85% Analysis Date = 10/21/14 SpikeMix = ERA 0227-14-06.1A: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 98% Analysis Date = 10/04/14 SpikeMix = Crescent 03DD004: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 105% Analysis Date = 07/11/14 SpikeMix = Spex Organics C1140417015: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 96% Analysis Date = 09/09/14 SpikeMix = Accu 214031115: 10 µl & NSI 032614: 10 µl Pct Recovery = 117% Analysis Date = 09/09/14 SpikeMix = NSI 032614: 10 µl & Spex Organics C1140417015: 10 µl Pct Recovery = 113% Analysis Date = 07/29/14 SpikeMix = Crescent 03DD004: 10 µl & NSI 032614: 10 µl Pct Recovery = 106% Analysis Date = 05/30/14 SpikeMix = NSI 032614: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 137% Analysis Date = 03/17/16 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 94% Analysis Date = 01/27/16 SpikeMix = Crescent 04EE008: 10 µl & NSI 050515AVOC: 10 µl Pct Recovery = 103% Analysis Date = 12/10/15 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 104% Analysis Date = 09/03/15 SpikeMix = NSI 050515AVOC: 10 µl & Spex Organics EN150428007: 10 µl Pct Recovery = 91% Analysis Date = 11/20/15 SpikeMix = Accu 215041380: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 103% Analysis Date = 07/31/15 SpikeMix = Crescent 04EE008: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 115% Analysis Date = 06/27/15 SpikeMix = ERA 0406-15-03: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 118% Analysis Date = 11/20/16 Pct Recovery = 123% Analysis Date = 11/16/16 Pct Recovery = 123% Analysis Date = 11/16/16 Pct Recovery = 123% Analysis Date = 11/11/16 Pct Recovery = 123% Analysis Date = 11/11/16 Pct Recovery = 123% Analysis Date = 11/06/16 Pct Recovery = 122% Analysis Date = 11/06/16 Pct Recovery = 122% Analysis Date = 11/02/16 Pct Recovery = 122% Analysis Date = 11/02/16 Pct Recovery = 122% Analysis Date = 10/28/16 Pct Recovery = 121% Analysis Date = 10/28/16 Pct Recovery = 121% Analysis Date = 10/23/16 Pct Recovery = 121% Analysis Date = 10/23/16 Pct Recovery = 121% Analysis Date = 10/19/16 Pct Recovery = 121% Analysis Date = 10/19/16 Pct Recovery = 121% Analysis Date = 10/14/16 Pct Recovery = 120% Analysis Date = 10/14/16 Pct Recovery = 120% Analysis Date = 10/09/16 Pct Recovery = 120% Analysis Date = 10/09/16 Pct Recovery = 120% Analysis Date = 10/05/16 Pct Recovery = 120% Analysis Date = 10/05/16 Pct Recovery = 120% Analysis Date = 09/30/16 Pct Recovery = 119% Analysis Date = 09/30/16 Pct Recovery = 119% Analysis Date = 09/25/16 Pct Recovery = 119% Analysis Date = 09/25/16 Pct Recovery = 119% Analysis Date = 09/21/16 Pct Recovery = 119% Analysis Date = 09/21/16 Pct Recovery = 119% Analysis Date = 09/16/16 Pct Recovery = 118% Analysis Date = 09/16/16 Pct Recovery = 118% Analysis Date = 09/11/16 Pct Recovery = 118% Analysis Date = 09/11/16 Pct Recovery = 118% Analysis Date = 09/07/16 Pct Recovery = 118% Analysis Date = 09/07/16 Pct Recovery = 118% Analysis Date = 09/02/16 Pct Recovery = 118% Analysis Date = 09/02/16 Pct Recovery = 118% Analysis Date = 08/28/16 Pct Recovery = 117% Analysis Date = 08/28/16 Pct Recovery = 117% Analysis Date = 08/24/16 Pct Recovery = 117% Analysis Date = 08/24/16 Pct Recovery = 117% Analysis Date = 08/19/16 Pct Recovery = 117% Analysis Date = 08/19/16 Pct Recovery = 117% Analysis Date = 08/14/16 Pct Recovery = 116% Analysis Date = 08/14/16 Pct Recovery = 116% Analysis Date = 08/10/16 Pct Recovery = 116% Analysis Date = 08/10/16 Pct Recovery = 116% Analysis Date = 08/05/16 Pct Recovery = 116% Analysis Date = 08/05/16 Pct Recovery = 116% Analysis Date = 07/31/16 Pct Recovery = 115% Analysis Date = 07/31/16 Pct Recovery = 115% Analysis Date = 07/27/16 Pct Recovery = 115% Analysis Date = 07/27/16 Pct Recovery = 115% Analysis Date = 07/22/16 Pct Recovery = 115% Analysis Date = 07/22/16 Pct Recovery = 115% Analysis Date = 07/17/16 Pct Recovery = 115% Analysis Date = 07/17/16 Pct Recovery = 115% Analysis Date = 07/13/16 Pct Recovery = 114% Analysis Date = 07/13/16 Pct Recovery = 114% Analysis Date = 07/08/16 Pct Recovery = 114% Analysis Date = 07/08/16 Pct Recovery = 114% Analysis Date = 07/03/16 Pct Recovery = 114% Analysis Date = 07/03/16 Pct Recovery = 114% Analysis Date = 06/29/16 Pct Recovery = 113% Analysis Date = 06/29/16 Pct Recovery = 113% Analysis Date = 06/24/16 Pct Recovery = 113% Analysis Date = 06/24/16 Pct Recovery = 113% Analysis Date = 06/19/16 Pct Recovery = 113% Analysis Date = 06/19/16 Pct Recovery = 113% Analysis Date = 06/15/16 Pct Recovery = 112% Analysis Date = 06/15/16 Pct Recovery = 112% Analysis Date = 06/10/16 Pct Recovery = 112% Analysis Date = 06/10/16 Pct Recovery = 112% Analysis Date = 06/05/16 Pct Recovery = 112% Analysis Date = 06/05/16 Pct Recovery = 112% Analysis Date = 06/01/16 Pct Recovery = 112% Analysis Date = 06/01/16 Pct Recovery = 112% Analysis Date = 05/27/16 Pct Recovery = 111% Analysis Date = 05/27/16 Pct Recovery = 111% Analysis Date = 05/22/16 Pct Recovery = 111% Analysis Date = 05/22/16 Pct Recovery = 111% Analysis Date = 05/17/16 Pct Recovery = 111% Analysis Date = 05/17/16 Pct Recovery = 111% Analysis Date = 05/13/16 Pct Recovery = 110% Analysis Date = 05/13/16 Pct Recovery = 110% Analysis Date = 05/08/16 Pct Recovery = 110% Analysis Date = 05/08/16 Pct Recovery = 110% Analysis Date = 05/03/16 Pct Recovery = 110% Analysis Date = 05/03/16 Pct Recovery = 110% Analysis Date = 04/29/16 Pct Recovery = 109% Analysis Date = 04/29/16 Pct Recovery = 109% Analysis Date = 04/24/16 Pct Recovery = 109% Analysis Date = 04/24/16 Pct Recovery = 109% Analysis Date = 04/19/16 Pct Recovery = 109% Analysis Date = 04/19/16 Pct Recovery = 109% Analysis Date = 04/15/16 Pct Recovery = 108% Analysis Date = 04/15/16 Pct Recovery = 108% Analysis Date = 04/10/16 Pct Recovery = 108% Analysis Date = 04/10/16 Pct Recovery = 108% Analysis Date = 04/05/16 Pct Recovery = 108% Analysis Date = 04/05/16 Pct Recovery = 108% Analysis Date = 04/01/16 Pct Recovery = 108% Analysis Date = 04/01/16 Pct Recovery = 108% Analysis Date = 03/27/16 Pct Recovery = 107% Analysis Date = 03/27/16 Pct Recovery = 107% Analysis Date = 03/22/16 Pct Recovery = 107% Analysis Date = 03/22/16 Pct Recovery = 107% Analysis Date = 03/18/16 Pct Recovery = 107% Analysis Date = 03/18/16 Pct Recovery = 107% Analysis Date = 03/13/16 Pct Recovery = 106% Analysis Date = 03/13/16 Pct Recovery = 106% Analysis Date = 03/08/16 Pct Recovery = 106% Analysis Date = 03/08/16 Pct Recovery = 106% Analysis Date = 03/04/16 Pct Recovery = 106% Analysis Date = 03/04/16 Pct Recovery = 106% Analysis Date = 02/28/16 Pct Recovery = 105% Analysis Date = 02/28/16 Pct Recovery = 105% Analysis Date = 02/23/16 Pct Recovery = 105% Analysis Date = 02/23/16 Pct Recovery = 105% Analysis Date = 02/19/16 Pct Recovery = 105% Analysis Date = 02/19/16 Pct Recovery = 105% Analysis Date = 02/14/16 Pct Recovery = 104% Analysis Date = 02/14/16 Pct Recovery = 104% Analysis Date = 02/09/16 Pct Recovery = 104% Analysis Date = 02/09/16 Pct Recovery = 104% Analysis Date = 02/05/16 Pct Recovery = 104% Analysis Date = 02/05/16 Pct Recovery = 104% Analysis Date = 01/31/16 Pct Recovery = 103% Analysis Date = 01/31/16 Pct Recovery = 103% Analysis Date = 01/26/16 Pct Recovery = 103% Analysis Date = 01/26/16 Pct Recovery = 103% Analysis Date = 01/22/16 Pct Recovery = 103% Analysis Date = 01/22/16 Pct Recovery = 103% Analysis Date = 01/17/16 Pct Recovery = 103% Analysis Date = 01/17/16 Pct Recovery = 103% Analysis Date = 01/12/16 Pct Recovery = 103% Analysis Date = 01/12/16 Pct Recovery = 103% Analysis Date = 01/08/16 Pct Recovery = 103% Analysis Date = 01/08/16 Pct Recovery = 103% Analysis Date = 01/03/16 Pct Recovery = 103% Analysis Date = 01/03/16 Pct Recovery = 103% Analysis Date = 12/29/15 Pct Recovery = 103% Analysis Date = 12/29/15 Pct Recovery = 103% Analysis Date = 12/25/15 Pct Recovery = 103% Analysis Date = 12/25/15 Pct Recovery = 103% Analysis Date = 12/20/15 Pct Recovery = 103% Analysis Date = 12/20/15 Pct Recovery = 103% Analysis Date = 12/15/15 Pct Recovery = 103% Analysis Date = 12/15/15 Pct Recovery = 103% Analysis Date = 12/11/15 Pct Recovery = 103% Analysis Date = 12/11/15 Pct Recovery = 103% Analysis Date = 12/06/15 Pct Recovery = 103% Analysis Date = 12/06/15 Pct Recovery = 103% Analysis Date = 12/01/15 Pct Recovery = 103% Analysis Date = 12/01/15 Pct Recovery = 103% Analysis Date = 11/27/15 Pct Recovery = 103% Analysis Date = 11/27/15 Pct Recovery = 103% Analysis Date = 11/22/15 Pct Recovery = 103% Analysis Date = 11/22/15 Pct Recovery = 103% Analysis Date = 11/17/15 Pct Recovery = 103% Analysis Date = 11/17/15 Pct Recovery = 103% Analysis Date = 11/12/15 Pct Recovery = 103% Analysis Date = 11/12/15 Pct Recovery = 103% Analysis Date = 11/08/15 Pct Recovery = 103% Analysis Date = 11/08/15 Pct Recovery = 103% Analysis Date = 11/03/15 Pct Recovery = 103% Analysis Date = 11/03/15 Pct Recovery = 103% Analysis Date = 10/29/15 Pct Recovery = 103% Analysis Date = 10/29/15 Pct Recovery = 103% Analysis Date = 10/25/15 Pct Recovery = 103% Analysis Date = 10/25/15 Pct Recovery = 103% Analysis Date = 10/20/15 Pct Recovery = 103% Analysis Date = 10/20/15 Pct Recovery = 103% Analysis Date = 10/15/15 Pct Recovery = 103% Analysis Date = 10/15/15 Pct Recovery = 103% Analysis Date = 10/11/15 Pct Recovery = 103% Analysis Date = 10/11/15 Pct Recovery = 103% Analysis Date = 10/06/15 Pct Recovery = 103% Analysis Date = 10/06/15 Pct Recovery = 103% Analysis Date = 10/01/15 Pct Recovery = 103% Analysis Date = 10/01/15 Pct Recovery = 103% Analysis Date = 09/27/15 Pct Recovery = 102% Analysis Date = 09/27/15 Pct Recovery = 102% Analysis Date = 09/22/15 Pct Recovery = 102% Analysis Date = 09/22/15 Pct Recovery = 102% Analysis Date = 09/17/15 Pct Recovery = 102% Analysis Date = 09/17/15 Pct Recovery = 102% Analysis Date = 09/13/15 Pct Recovery = 102% Analysis Date = 09/13/15 Pct Recovery = 102% Analysis Date = 09/08/15 Pct Recovery = 102% Analysis Date = 09/08/15 Pct Recovery = 102% Analysis Date = 09/03/15 Pct Recovery = 102% Analysis Date = 09/03/15 Pct Recovery = 102% Analysis Date = 08/30/15 Pct Recovery = 102% Analysis Date = 08/30/15 Pct Recovery = 102% Analysis Date = 08/25/15 Pct Recovery = 102% Analysis Date = 08/25/15 Pct Recovery = 102% Analysis Date = 08/20/15 Pct Recovery = 102% Analysis Date = 08/20/15 Pct Recovery = 102% Analysis Date = 08/16/15 Pct Recovery = 102% Analysis Date = 08/16/15 Pct Recovery = 102% Analysis Date = 08/11/15 Pct Recovery = 102% Analysis Date = 08/11/15 Pct Recovery = 102% Analysis Date = 08/06/15 Pct Recovery = 102% Analysis Date = 08/06/15 Pct Recovery = 102% Analysis Date = 08/02/15 Pct Recovery = 102% Analysis Date = 08/02/15 Pct Recovery = 102% Analysis Date = 07/28/15 Pct Recovery = 102% Analysis Date = 07/28/15 Pct Recovery = 102% Analysis Date = 07/23/15 Pct Recovery = 101% Analysis Date = 07/23/15 Pct Recovery = 101% Analysis Date = 07/19/15 Pct Recovery = 101% Analysis Date = 07/19/15 Pct Recovery = 101% Analysis Date = 07/14/15 Pct Recovery = 101% Analysis Date = 07/14/15 Pct Recovery = 101% Analysis Date = 07/09/15 Pct Recovery = 101% Analysis Date = 07/09/15 Pct Recovery = 101% Analysis Date = 07/05/15 Pct Recovery = 101% Analysis Date = 07/05/15 Pct Recovery = 101% Analysis Date = 06/30/15 Pct Recovery = 101% Analysis Date = 06/30/15 Pct Recovery = 101% Analysis Date = 06/25/15 Pct Recovery = 101% Analysis Date = 06/25/15 Pct Recovery = 101% Analysis Date = 06/21/15 Pct Recovery = 101% Analysis Date = 06/21/15 Pct Recovery = 101% Analysis Date = 06/16/15 Pct Recovery = 101% Analysis Date = 06/16/15 Pct Recovery = 101% Analysis Date = 06/11/15 Pct Recovery = 101% Analysis Date = 06/11/15 Pct Recovery = 101% Analysis Date = 06/07/15 Pct Recovery = 100% Analysis Date = 06/07/15 Pct Recovery = 100% Analysis Date = 06/02/15 Pct Recovery = 100% Analysis Date = 06/02/15 Pct Recovery = 100% Analysis Date = 05/28/15 Pct Recovery = 100% Analysis Date = 05/28/15 Pct Recovery = 100% Analysis Date = 05/24/15 Pct Recovery = 100% Analysis Date = 05/24/15 Pct Recovery = 100% Analysis Date = 05/19/15 Pct Recovery = 100% Analysis Date = 05/19/15 Pct Recovery = 100% Analysis Date = 05/14/15 Pct Recovery = 100% Analysis Date = 05/14/15 Pct Recovery = 100% Analysis Date = 05/09/15 Pct Recovery = 100% Analysis Date = 05/09/15 Pct Recovery = 100% Analysis Date = 05/05/15 Pct Recovery = 100% Analysis Date = 05/05/15 Pct Recovery = 100% Analysis Date = 04/30/15 Pct Recovery = 100% Analysis Date = 04/30/15 Pct Recovery = 100% Analysis Date = 04/25/15 Pct Recovery = 100% Analysis Date = 04/25/15 Pct Recovery = 100% Analysis Date = 04/21/15 Pct Recovery = 100% Analysis Date = 04/21/15 Pct Recovery = 100% Analysis Date = 04/16/15 Pct Recovery = 100% Analysis Date = 04/16/15 Pct Recovery = 100% Analysis Date = 04/11/15 Pct Recovery = 100% Analysis Date = 04/11/15 Pct Recovery = 100% Analysis Date = 04/07/15 Pct Recovery = 100% Analysis Date = 04/07/15 Pct Recovery = 100% Analysis Date = 04/02/15 Pct Recovery = 100% Analysis Date = 04/02/15 Pct Recovery = 100% Analysis Date = 03/28/15 Pct Recovery = 100% Analysis Date = 03/28/15 Pct Recovery = 100% Analysis Date = 03/24/15 Pct Recovery = 100% Analysis Date = 03/24/15 Pct Recovery = 100% Analysis Date = 03/19/15 Pct Recovery = 100% Analysis Date = 03/19/15 Pct Recovery = 100% Analysis Date = 03/14/15 Pct Recovery = 100% Analysis Date = 03/14/15 Pct Recovery = 100% Analysis Date = 03/10/15 Pct Recovery = 100% Analysis Date = 03/10/15 Pct Recovery = 100% Analysis Date = 03/05/15 Pct Recovery = 100% Analysis Date = 03/05/15 Pct Recovery = 100% Analysis Date = 02/28/15 Pct Recovery = 100% Analysis Date = 02/28/15 Pct Recovery = 100% Analysis Date = 02/24/15 Pct Recovery = 100% Analysis Date = 02/24/15 Pct Recovery = 100% Analysis Date = 02/19/15 Pct Recovery = 100% Analysis Date = 02/19/15 Pct Recovery = 100% Analysis Date = 02/14/15 Pct Recovery = 100% Analysis Date = 02/14/15 Pct Recovery = 100% Analysis Date = 02/10/15 Pct Recovery = 100% Analysis Date = 02/10/15 Pct Recovery = 100% Analysis Date = 02/05/15 Pct Recovery = 100% Analysis Date = 02/05/15 Pct Recovery = 100% Analysis Date = 01/31/15 Pct Recovery = 100% Analysis Date = 01/31/15 Pct Recovery = 100% Analysis Date = 01/27/15 Pct Recovery = 100% Analysis Date = 01/27/15 Pct Recovery = 100% Analysis Date = 01/22/15 Pct Recovery = 100% Analysis Date = 01/22/15 Pct Recovery = 100% Analysis Date = 01/17/15 Pct Recovery = 100% Analysis Date = 01/17/15 Pct Recovery = 100% Analysis Date = 01/13/15 Pct Recovery = 100% Analysis Date = 01/13/15 Pct Recovery = 100% Analysis Date = 01/08/15 Pct Recovery = 100% Analysis Date = 01/08/15 Pct Recovery = 100% Analysis Date = 01/03/15 Pct Recovery = 100% Analysis Date = 01/03/15 Pct Recovery = 100% Analysis Date = 12/30/14 Pct Recovery = 100% Analysis Date = 12/30/14 Pct Recovery = 100% Analysis Date = 12/25/14 Pct Recovery = 100% Analysis Date = 12/25/14 Pct Recovery = 100% Analysis Date = 12/20/14 Pct Recovery = 100% Analysis Date = 12/20/14 Pct Recovery = 100% Analysis Date = 12/16/14 Pct Recovery = 100% Analysis Date = 12/16/14 Pct Recovery = 100% Analysis Date = 12/11/14 Pct Recovery = 101% Analysis Date = 12/11/14 Pct Recovery = 101% Analysis Date = 12/06/14 Pct Recovery = 101% Analysis Date = 12/06/14 Pct Recovery = 101% Analysis Date = 12/02/14 Pct Recovery = 101% Analysis Date = 12/02/14 Pct Recovery = 101% Analysis Date = 11/27/14 Pct Recovery = 101% Analysis Date = 11/27/14 Pct Recovery = 101% Analysis Date = 11/22/14 Pct Recovery = 101% Analysis Date = 11/22/14 Pct Recovery = 101% Analysis Date = 11/18/14 Pct Recovery = 101% Analysis Date = 11/18/14 Pct Recovery = 101% Analysis Date = 11/13/14 Pct Recovery = 101% Analysis Date = 11/13/14 Pct Recovery = 101% Analysis Date = 11/08/14 Pct Recovery = 101% Analysis Date = 11/08/14 Pct Recovery = 101% Analysis Date = 11/03/14 Pct Recovery = 102% Analysis Date = 11/03/14 Pct Recovery = 102% Analysis Date = 10/30/14 Pct Recovery = 102% Analysis Date = 10/30/14 Pct Recovery = 102% Analysis Date = 10/25/14 Pct Recovery = 102% Analysis Date = 10/25/14 Pct Recovery = 102% Analysis Date = 10/20/14 Pct Recovery = 102% Analysis Date = 10/20/14 Pct Recovery = 102% Analysis Date = 10/16/14 Pct Recovery = 102% Analysis Date = 10/16/14 Pct Recovery = 102% Analysis Date = 10/11/14 Pct Recovery = 102% Analysis Date = 10/11/14 Pct Recovery = 102% Analysis Date = 10/06/14 Pct Recovery = 103% Analysis Date = 10/06/14 Pct Recovery = 103% Analysis Date = 10/02/14 Pct Recovery = 103% Analysis Date = 10/02/14 Pct Recovery = 103% Analysis Date = 09/27/14 Pct Recovery = 103% Analysis Date = 09/27/14 Pct Recovery = 103% Analysis Date = 09/22/14 Pct Recovery = 103% Analysis Date = 09/22/14 Pct Recovery = 103% Analysis Date = 09/18/14 Pct Recovery = 103% Analysis Date = 09/18/14 Pct Recovery = 103% Analysis Date = 09/13/14 Pct Recovery = 103% Analysis Date = 09/13/14 Pct Recovery = 103% Analysis Date = 09/08/14 Pct Recovery = 103% Analysis Date = 09/08/14 Pct Recovery = 103% Analysis Date = 09/04/14 Pct Recovery = 104% Analysis Date = 09/04/14 Pct Recovery = 104% Analysis Date = 08/30/14 Pct Recovery = 104% Analysis Date = 08/30/14 Pct Recovery = 104% Analysis Date = 08/25/14 Pct Recovery = 104% Analysis Date = 08/25/14 Pct Recovery = 104% Analysis Date = 08/21/14 Pct Recovery = 104% Analysis Date = 08/21/14 Pct Recovery = 104% Analysis Date = 08/16/14 Pct Recovery = 104% Analysis Date = 08/16/14 Pct Recovery = 104% Analysis Date = 08/11/14 Pct Recovery = 105% Analysis Date = 08/11/14 Pct Recovery = 105% Analysis Date = 08/07/14 Pct Recovery = 105% Analysis Date = 08/07/14 Pct Recovery = 105% Analysis Date = 08/02/14 Pct Recovery = 105% Analysis Date = 08/02/14 Pct Recovery = 105% Analysis Date = 07/28/14 Pct Recovery = 105% Analysis Date = 07/28/14 Pct Recovery = 105% Analysis Date = 07/24/14 Pct Recovery = 105% Analysis Date = 07/24/14 Pct Recovery = 105% Analysis Date = 07/19/14 Pct Recovery = 105% Analysis Date = 07/19/14 Pct Recovery = 105% Analysis Date = 07/14/14 Pct Recovery = 106% Analysis Date = 07/14/14 Pct Recovery = 106% Analysis Date = 07/10/14 Pct Recovery = 106% Analysis Date = 07/10/14 Pct Recovery = 106% Analysis Date = 07/05/14 Pct Recovery = 106% Analysis Date = 07/05/14 Pct Recovery = 106% Analysis Date = 06/30/14 Pct Recovery = 106% Analysis Date = 06/30/14 Pct Recovery = 106% Analysis Date = 06/26/14 Pct Recovery = 106% Analysis Date = 06/26/14 Pct Recovery = 106% Analysis Date = 06/21/14 Pct Recovery = 107% Analysis Date = 06/21/14 Pct Recovery = 107% Analysis Date = 06/16/14 Pct Recovery = 107% Analysis Date = 06/16/14 Pct Recovery = 107% Analysis Date = 06/12/14 Pct Recovery = 107% Analysis Date = 06/12/14 Pct Recovery = 107% Analysis Date = 06/07/14 Pct Recovery = 107% Analysis Date = 06/07/14 Pct Recovery = 107% Analysis Date = 06/02/14 Pct Recovery = 108% Analysis Date = 06/02/14 Pct Recovery = 108% Analysis Date = 05/29/14 Pct Recovery = 108% Analysis Date = 05/29/14 Pct Recovery = 108% Analysis Date = 05/24/14 Pct Recovery = 108% Analysis Date = 05/24/14 Pct Recovery = 108% Analysis Date = 05/19/14 Pct Recovery = 108% Analysis Date = 05/19/14 Pct Recovery = 108% Analysis Date = 05/15/14 Pct Recovery = 108% Analysis Date = 05/15/14 Pct Recovery = 108% Analysis Date = 05/10/14 Pct Recovery = 109% Analysis Date = 05/10/14 Pct Recovery = 109% Analysis Date = 05/05/14 Pct Recovery = 109% Analysis Date = 05/05/14 Pct Recovery = 109% Analysis Date = 05/01/14 Pct Recovery = 109% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
TRANS-1,2-DICHLOROETHYLENE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 40 105% 15% 103% 8%
Total 40 105% 15% 103% 8%

Sample Statistics
TRANS-1,2-DICHLOROETHYLENE

Characteristic N % % Basis
Plotted 40 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 40 .  
False Negatives 0 0% 0 out of 40
Not Spiked 25 .  
False Positives 3 12% 3 out of 25

BQS OBSP Determination:
TRANS-1,3-DICHLOROPROPENE
METHOD: 4440 , TESTIDCODE: 34699GCM66
Open Data Set

Analysis Date = 12/16/16 SpikeMix = NSI 041816AVOC: 40 µl & ChemService 5082900: 40 µl Pct Recovery = 93% Analysis Date = 07/14/16 SpikeMix = Accu 216041125: 40 µl & NSI 041816AVOC: 40 µl Pct Recovery = 98% Analysis Date = 12/12/16 SpikeMix = Accu 216041125: 40 µl & Crescent 03FF058: 40 µl Pct Recovery = 98% Analysis Date = 08/04/16 SpikeMix = Crescent 03FF058: 40 µl & Supelco LC20141V: 40 µl Pct Recovery = 81% Analysis Date = 08/26/16 SpikeMix = NSI 041816AVOC: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 82% Analysis Date = 11/21/16 SpikeMix = Crescent 03FF058: 25 µl & Supelco LC20141V: 25 µl Pct Recovery = 84% Analysis Date = 06/30/16 SpikeMix = Crescent 03FF058: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 86% Analysis Date = 06/21/16 SpikeMix = Phenova B20160319: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 90% Analysis Date = 05/24/16 SpikeMix = Accu 216041125: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 87% Analysis Date = 09/29/15 SpikeMix = Accu 215041380: 25 µl & ERA 0406-15-03: 25 µl Pct Recovery = 69% Analysis Date = 08/15/15 SpikeMix = Supelco LC13545: 25 µl & Crescent 04EE008: 25 µl Pct Recovery = 87% Analysis Date = 07/13/15 SpikeMix = Crescent 04EE008: 25 µl & NSI 050515AVOC: 25 µl Pct Recovery = 89% Analysis Date = 03/06/15 SpikeMix = ERA 0227-14-06.1A: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 83% Analysis Date = 12/17/14 SpikeMix = Supelco LC06438: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 91% Analysis Date = 09/21/14 SpikeMix = Supelco LC06438: 20 µl Pct Recovery = 98% Analysis Date = 06/10/14 SpikeMix = NSI 032614: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 91% Analysis Date = 03/19/15 SpikeMix = Spex Organics C1140417015: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 98% Analysis Date = 11/22/14 SpikeMix = NSI 032614: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 118% Analysis Date = 08/19/14 SpikeMix = Spex Organics C1140417015: 20 µl & Accu 214031115: 20 µl Pct Recovery = 95% Analysis Date = 08/16/14 SpikeMix = ERA 0227-14-06.1A: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 93% Analysis Date = 10/13/16 SpikeMix = Accu 216041125: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 120% Analysis Date = 10/13/16 SpikeMix = NSI 041816AVOC: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 113% Analysis Date = 07/29/16 SpikeMix = Phenova B20160319: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 120% Analysis Date = 06/15/16 SpikeMix = NSI 041816AVOC: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 97% Analysis Date = 09/28/16 SpikeMix = Crescent 03FF058: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 100% Analysis Date = 09/08/16 SpikeMix = Phenova B20160319: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 93% Analysis Date = 08/20/16 SpikeMix = Accu 216041125: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 113% Analysis Date = 04/02/16 SpikeMix = Supelco LC13545: 15 µl & Accu 215041380: 15 µl Pct Recovery = 89% Analysis Date = 03/04/16 SpikeMix = Accu 215041380: 15 µl & ERA 0406-15-03: 15 µl Pct Recovery = 106% Analysis Date = 06/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Accu 215041380: 15 µl Pct Recovery = 73% Analysis Date = 12/18/15 SpikeMix = Supelco LC13545: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 108% Analysis Date = 10/17/15 SpikeMix = Crescent 04EE008: 15 µl & NSI 050515AVOC: 15 µl Pct Recovery = 99% Analysis Date = 05/09/15 SpikeMix = Spex Organics EN150428007: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 92% Analysis Date = 10/21/14 SpikeMix = ERA 0227-14-06.1A: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 92% Analysis Date = 06/18/14 SpikeMix = Supelco LC06438: 10 µl & Accu 214031115: 10 µl Pct Recovery = 111% Analysis Date = 05/30/14 SpikeMix = NSI 032614: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 108% Analysis Date = 05/03/14 SpikeMix = Crescent 03DD004: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 99% Analysis Date = 11/06/14 SpikeMix = Spex Organics C1140417015: 10 µl & Crescent 03DD004: 10 µl Pct Recovery = 111% Analysis Date = 09/09/14 SpikeMix = NSI 032614: 10 µl & Spex Organics C1140417015: 10 µl Pct Recovery = 126% Analysis Date = 07/23/14 SpikeMix = Spex Organics C1140417015: 10 µl & Accu 214031115: 10 µl Pct Recovery = 109% Analysis Date = 07/11/14 SpikeMix = Spex Organics C1140417015: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 98% Analysis Date = 02/18/16 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 107% Analysis Date = 11/20/15 SpikeMix = Accu 215041380: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 88% Analysis Date = 11/12/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 93% Analysis Date = 05/21/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 95% Analysis Date = 05/13/16 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 114% Analysis Date = 01/27/16 SpikeMix = Crescent 04EE008: 10 µl & NSI 050515AVOC: 10 µl Pct Recovery = 80% Analysis Date = 08/07/15 SpikeMix = Crescent 04EE008: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 77% Analysis Date = 05/09/15 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 83% Analysis Date = 12/16/16 Pct Recovery = 99% Analysis Date = 12/11/16 Pct Recovery = 99% Analysis Date = 12/11/16 Pct Recovery = 99% Analysis Date = 12/06/16 Pct Recovery = 99% Analysis Date = 12/06/16 Pct Recovery = 99% Analysis Date = 12/01/16 Pct Recovery = 99% Analysis Date = 12/01/16 Pct Recovery = 99% Analysis Date = 11/26/16 Pct Recovery = 99% Analysis Date = 11/26/16 Pct Recovery = 99% Analysis Date = 11/22/16 Pct Recovery = 99% Analysis Date = 11/22/16 Pct Recovery = 99% Analysis Date = 11/17/16 Pct Recovery = 99% Analysis Date = 11/17/16 Pct Recovery = 99% Analysis Date = 11/12/16 Pct Recovery = 99% Analysis Date = 11/12/16 Pct Recovery = 99% Analysis Date = 11/07/16 Pct Recovery = 99% Analysis Date = 11/07/16 Pct Recovery = 99% Analysis Date = 11/02/16 Pct Recovery = 99% Analysis Date = 11/02/16 Pct Recovery = 99% Analysis Date = 10/29/16 Pct Recovery = 99% Analysis Date = 10/29/16 Pct Recovery = 99% Analysis Date = 10/24/16 Pct Recovery = 99% Analysis Date = 10/24/16 Pct Recovery = 99% Analysis Date = 10/19/16 Pct Recovery = 99% Analysis Date = 10/19/16 Pct Recovery = 99% Analysis Date = 10/14/16 Pct Recovery = 99% Analysis Date = 10/14/16 Pct Recovery = 99% Analysis Date = 10/09/16 Pct Recovery = 99% Analysis Date = 10/09/16 Pct Recovery = 99% Analysis Date = 10/05/16 Pct Recovery = 99% Analysis Date = 10/05/16 Pct Recovery = 99% Analysis Date = 09/30/16 Pct Recovery = 99% Analysis Date = 09/30/16 Pct Recovery = 99% Analysis Date = 09/25/16 Pct Recovery = 98% Analysis Date = 09/25/16 Pct Recovery = 98% Analysis Date = 09/20/16 Pct Recovery = 98% Analysis Date = 09/20/16 Pct Recovery = 98% Analysis Date = 09/15/16 Pct Recovery = 98% Analysis Date = 09/15/16 Pct Recovery = 98% Analysis Date = 09/11/16 Pct Recovery = 98% Analysis Date = 09/11/16 Pct Recovery = 98% Analysis Date = 09/06/16 Pct Recovery = 98% Analysis Date = 09/06/16 Pct Recovery = 98% Analysis Date = 09/01/16 Pct Recovery = 98% Analysis Date = 09/01/16 Pct Recovery = 98% Analysis Date = 08/27/16 Pct Recovery = 98% Analysis Date = 08/27/16 Pct Recovery = 98% Analysis Date = 08/23/16 Pct Recovery = 98% Analysis Date = 08/23/16 Pct Recovery = 98% Analysis Date = 08/18/16 Pct Recovery = 98% Analysis Date = 08/18/16 Pct Recovery = 98% Analysis Date = 08/13/16 Pct Recovery = 98% Analysis Date = 08/13/16 Pct Recovery = 98% Analysis Date = 08/08/16 Pct Recovery = 98% Analysis Date = 08/08/16 Pct Recovery = 98% Analysis Date = 08/03/16 Pct Recovery = 98% Analysis Date = 08/03/16 Pct Recovery = 98% Analysis Date = 07/30/16 Pct Recovery = 98% Analysis Date = 07/30/16 Pct Recovery = 98% Analysis Date = 07/25/16 Pct Recovery = 98% Analysis Date = 07/25/16 Pct Recovery = 98% Analysis Date = 07/20/16 Pct Recovery = 98% Analysis Date = 07/20/16 Pct Recovery = 98% Analysis Date = 07/15/16 Pct Recovery = 98% Analysis Date = 07/15/16 Pct Recovery = 98% Analysis Date = 07/10/16 Pct Recovery = 98% Analysis Date = 07/10/16 Pct Recovery = 98% Analysis Date = 07/06/16 Pct Recovery = 98% Analysis Date = 07/06/16 Pct Recovery = 98% Analysis Date = 07/01/16 Pct Recovery = 98% Analysis Date = 07/01/16 Pct Recovery = 98% Analysis Date = 06/26/16 Pct Recovery = 98% Analysis Date = 06/26/16 Pct Recovery = 98% Analysis Date = 06/21/16 Pct Recovery = 98% Analysis Date = 06/21/16 Pct Recovery = 98% Analysis Date = 06/16/16 Pct Recovery = 97% Analysis Date = 06/16/16 Pct Recovery = 97% Analysis Date = 06/12/16 Pct Recovery = 97% Analysis Date = 06/12/16 Pct Recovery = 97% Analysis Date = 06/07/16 Pct Recovery = 97% Analysis Date = 06/07/16 Pct Recovery = 97% Analysis Date = 06/02/16 Pct Recovery = 97% Analysis Date = 06/02/16 Pct Recovery = 97% Analysis Date = 05/28/16 Pct Recovery = 97% Analysis Date = 05/28/16 Pct Recovery = 97% Analysis Date = 05/24/16 Pct Recovery = 97% Analysis Date = 05/24/16 Pct Recovery = 97% Analysis Date = 05/19/16 Pct Recovery = 97% Analysis Date = 05/19/16 Pct Recovery = 97% Analysis Date = 05/14/16 Pct Recovery = 97% Analysis Date = 05/14/16 Pct Recovery = 97% Analysis Date = 05/09/16 Pct Recovery = 97% Analysis Date = 05/09/16 Pct Recovery = 97% Analysis Date = 05/04/16 Pct Recovery = 97% Analysis Date = 05/04/16 Pct Recovery = 97% Analysis Date = 04/30/16 Pct Recovery = 96% Analysis Date = 04/30/16 Pct Recovery = 96% Analysis Date = 04/25/16 Pct Recovery = 96% Analysis Date = 04/25/16 Pct Recovery = 96% Analysis Date = 04/20/16 Pct Recovery = 96% Analysis Date = 04/20/16 Pct Recovery = 96% Analysis Date = 04/15/16 Pct Recovery = 96% Analysis Date = 04/15/16 Pct Recovery = 96% Analysis Date = 04/10/16 Pct Recovery = 96% Analysis Date = 04/10/16 Pct Recovery = 96% Analysis Date = 04/06/16 Pct Recovery = 96% Analysis Date = 04/06/16 Pct Recovery = 96% Analysis Date = 04/01/16 Pct Recovery = 96% Analysis Date = 04/01/16 Pct Recovery = 96% Analysis Date = 03/27/16 Pct Recovery = 95% Analysis Date = 03/27/16 Pct Recovery = 95% Analysis Date = 03/22/16 Pct Recovery = 95% Analysis Date = 03/22/16 Pct Recovery = 95% Analysis Date = 03/17/16 Pct Recovery = 95% Analysis Date = 03/17/16 Pct Recovery = 95% Analysis Date = 03/13/16 Pct Recovery = 95% Analysis Date = 03/13/16 Pct Recovery = 95% Analysis Date = 03/08/16 Pct Recovery = 95% Analysis Date = 03/08/16 Pct Recovery = 95% Analysis Date = 03/03/16 Pct Recovery = 95% Analysis Date = 03/03/16 Pct Recovery = 95% Analysis Date = 02/27/16 Pct Recovery = 95% Analysis Date = 02/27/16 Pct Recovery = 95% Analysis Date = 02/23/16 Pct Recovery = 94% Analysis Date = 02/23/16 Pct Recovery = 94% Analysis Date = 02/18/16 Pct Recovery = 94% Analysis Date = 02/18/16 Pct Recovery = 94% Analysis Date = 02/13/16 Pct Recovery = 94% Analysis Date = 02/13/16 Pct Recovery = 94% Analysis Date = 02/08/16 Pct Recovery = 94% Analysis Date = 02/08/16 Pct Recovery = 94% Analysis Date = 02/03/16 Pct Recovery = 94% Analysis Date = 02/03/16 Pct Recovery = 94% Analysis Date = 01/30/16 Pct Recovery = 94% Analysis Date = 01/30/16 Pct Recovery = 94% Analysis Date = 01/25/16 Pct Recovery = 93% Analysis Date = 01/25/16 Pct Recovery = 93% Analysis Date = 01/20/16 Pct Recovery = 93% Analysis Date = 01/20/16 Pct Recovery = 93% Analysis Date = 01/15/16 Pct Recovery = 93% Analysis Date = 01/15/16 Pct Recovery = 93% Analysis Date = 01/10/16 Pct Recovery = 93% Analysis Date = 01/10/16 Pct Recovery = 93% Analysis Date = 01/06/16 Pct Recovery = 93% Analysis Date = 01/06/16 Pct Recovery = 93% Analysis Date = 01/01/16 Pct Recovery = 92% Analysis Date = 01/01/16 Pct Recovery = 92% Analysis Date = 12/27/15 Pct Recovery = 92% Analysis Date = 12/27/15 Pct Recovery = 92% Analysis Date = 12/22/15 Pct Recovery = 92% Analysis Date = 12/22/15 Pct Recovery = 92% Analysis Date = 12/17/15 Pct Recovery = 92% Analysis Date = 12/17/15 Pct Recovery = 92% Analysis Date = 12/13/15 Pct Recovery = 92% Analysis Date = 12/13/15 Pct Recovery = 92% Analysis Date = 12/08/15 Pct Recovery = 92% Analysis Date = 12/08/15 Pct Recovery = 92% Analysis Date = 12/03/15 Pct Recovery = 92% Analysis Date = 12/03/15 Pct Recovery = 92% Analysis Date = 11/28/15 Pct Recovery = 91% Analysis Date = 11/28/15 Pct Recovery = 91% Analysis Date = 11/24/15 Pct Recovery = 91% Analysis Date = 11/24/15 Pct Recovery = 91% Analysis Date = 11/19/15 Pct Recovery = 91% Analysis Date = 11/19/15 Pct Recovery = 91% Analysis Date = 11/14/15 Pct Recovery = 91% Analysis Date = 11/14/15 Pct Recovery = 91% Analysis Date = 11/09/15 Pct Recovery = 91% Analysis Date = 11/09/15 Pct Recovery = 91% Analysis Date = 11/04/15 Pct Recovery = 91% Analysis Date = 11/04/15 Pct Recovery = 91% Analysis Date = 10/31/15 Pct Recovery = 91% Analysis Date = 10/31/15 Pct Recovery = 91% Analysis Date = 10/26/15 Pct Recovery = 91% Analysis Date = 10/26/15 Pct Recovery = 91% Analysis Date = 10/21/15 Pct Recovery = 90% Analysis Date = 10/21/15 Pct Recovery = 90% Analysis Date = 10/16/15 Pct Recovery = 90% Analysis Date = 10/16/15 Pct Recovery = 90% Analysis Date = 10/11/15 Pct Recovery = 90% Analysis Date = 10/11/15 Pct Recovery = 90% Analysis Date = 10/07/15 Pct Recovery = 90% Analysis Date = 10/07/15 Pct Recovery = 90% Analysis Date = 10/02/15 Pct Recovery = 90% Analysis Date = 10/02/15 Pct Recovery = 90% Analysis Date = 09/27/15 Pct Recovery = 90% Analysis Date = 09/27/15 Pct Recovery = 90% Analysis Date = 09/22/15 Pct Recovery = 90% Analysis Date = 09/22/15 Pct Recovery = 90% Analysis Date = 09/17/15 Pct Recovery = 90% Analysis Date = 09/17/15 Pct Recovery = 90% Analysis Date = 09/13/15 Pct Recovery = 90% Analysis Date = 09/13/15 Pct Recovery = 90% Analysis Date = 09/08/15 Pct Recovery = 90% Analysis Date = 09/08/15 Pct Recovery = 90% Analysis Date = 09/03/15 Pct Recovery = 90% Analysis Date = 09/03/15 Pct Recovery = 90% Analysis Date = 08/29/15 Pct Recovery = 89% Analysis Date = 08/29/15 Pct Recovery = 89% Analysis Date = 08/25/15 Pct Recovery = 89% Analysis Date = 08/25/15 Pct Recovery = 89% Analysis Date = 08/20/15 Pct Recovery = 89% Analysis Date = 08/20/15 Pct Recovery = 89% Analysis Date = 08/15/15 Pct Recovery = 89% Analysis Date = 08/15/15 Pct Recovery = 89% Analysis Date = 08/10/15 Pct Recovery = 89% Analysis Date = 08/10/15 Pct Recovery = 89% Analysis Date = 08/05/15 Pct Recovery = 89% Analysis Date = 08/05/15 Pct Recovery = 89% Analysis Date = 08/01/15 Pct Recovery = 89% Analysis Date = 08/01/15 Pct Recovery = 89% Analysis Date = 07/27/15 Pct Recovery = 89% Analysis Date = 07/27/15 Pct Recovery = 89% Analysis Date = 07/22/15 Pct Recovery = 89% Analysis Date = 07/22/15 Pct Recovery = 89% Analysis Date = 07/17/15 Pct Recovery = 89% Analysis Date = 07/17/15 Pct Recovery = 89% Analysis Date = 07/12/15 Pct Recovery = 90% Analysis Date = 07/12/15 Pct Recovery = 90% Analysis Date = 07/08/15 Pct Recovery = 90% Analysis Date = 07/08/15 Pct Recovery = 90% Analysis Date = 07/03/15 Pct Recovery = 90% Analysis Date = 07/03/15 Pct Recovery = 90% Analysis Date = 06/28/15 Pct Recovery = 90% Analysis Date = 06/28/15 Pct Recovery = 90% Analysis Date = 06/23/15 Pct Recovery = 90% Analysis Date = 06/23/15 Pct Recovery = 90% Analysis Date = 06/18/15 Pct Recovery = 90% Analysis Date = 06/18/15 Pct Recovery = 90% Analysis Date = 06/14/15 Pct Recovery = 90% Analysis Date = 06/14/15 Pct Recovery = 90% Analysis Date = 06/09/15 Pct Recovery = 90% Analysis Date = 06/09/15 Pct Recovery = 90% Analysis Date = 06/04/15 Pct Recovery = 90% Analysis Date = 06/04/15 Pct Recovery = 90% Analysis Date = 05/30/15 Pct Recovery = 90% Analysis Date = 05/30/15 Pct Recovery = 90% Analysis Date = 05/25/15 Pct Recovery = 90% Analysis Date = 05/25/15 Pct Recovery = 90% Analysis Date = 05/21/15 Pct Recovery = 91% Analysis Date = 05/21/15 Pct Recovery = 91% Analysis Date = 05/16/15 Pct Recovery = 91% Analysis Date = 05/16/15 Pct Recovery = 91% Analysis Date = 05/11/15 Pct Recovery = 91% Analysis Date = 05/11/15 Pct Recovery = 91% Analysis Date = 05/06/15 Pct Recovery = 91% Analysis Date = 05/06/15 Pct Recovery = 91% Analysis Date = 05/02/15 Pct Recovery = 91% Analysis Date = 05/02/15 Pct Recovery = 91% Analysis Date = 04/27/15 Pct Recovery = 91% Analysis Date = 04/27/15 Pct Recovery = 91% Analysis Date = 04/22/15 Pct Recovery = 91% Analysis Date = 04/22/15 Pct Recovery = 91% Analysis Date = 04/17/15 Pct Recovery = 92% Analysis Date = 04/17/15 Pct Recovery = 92% Analysis Date = 04/12/15 Pct Recovery = 92% Analysis Date = 04/12/15 Pct Recovery = 92% Analysis Date = 04/08/15 Pct Recovery = 92% Analysis Date = 04/08/15 Pct Recovery = 92% Analysis Date = 04/03/15 Pct Recovery = 92% Analysis Date = 04/03/15 Pct Recovery = 92% Analysis Date = 03/29/15 Pct Recovery = 92% Analysis Date = 03/29/15 Pct Recovery = 92% Analysis Date = 03/24/15 Pct Recovery = 92% Analysis Date = 03/24/15 Pct Recovery = 92% Analysis Date = 03/19/15 Pct Recovery = 93% Analysis Date = 03/19/15 Pct Recovery = 93% Analysis Date = 03/15/15 Pct Recovery = 93% Analysis Date = 03/15/15 Pct Recovery = 93% Analysis Date = 03/10/15 Pct Recovery = 93% Analysis Date = 03/10/15 Pct Recovery = 93% Analysis Date = 03/05/15 Pct Recovery = 93% Analysis Date = 03/05/15 Pct Recovery = 93% Analysis Date = 02/28/15 Pct Recovery = 93% Analysis Date = 02/28/15 Pct Recovery = 93% Analysis Date = 02/23/15 Pct Recovery = 94% Analysis Date = 02/23/15 Pct Recovery = 94% Analysis Date = 02/19/15 Pct Recovery = 94% Analysis Date = 02/19/15 Pct Recovery = 94% Analysis Date = 02/14/15 Pct Recovery = 94% Analysis Date = 02/14/15 Pct Recovery = 94% Analysis Date = 02/09/15 Pct Recovery = 94% Analysis Date = 02/09/15 Pct Recovery = 94% Analysis Date = 02/04/15 Pct Recovery = 94% Analysis Date = 02/04/15 Pct Recovery = 94% Analysis Date = 01/31/15 Pct Recovery = 95% Analysis Date = 01/31/15 Pct Recovery = 95% Analysis Date = 01/26/15 Pct Recovery = 95% Analysis Date = 01/26/15 Pct Recovery = 95% Analysis Date = 01/21/15 Pct Recovery = 95% Analysis Date = 01/21/15 Pct Recovery = 95% Analysis Date = 01/16/15 Pct Recovery = 95% Analysis Date = 01/16/15 Pct Recovery = 95% Analysis Date = 01/11/15 Pct Recovery = 95% Analysis Date = 01/11/15 Pct Recovery = 95% Analysis Date = 01/07/15 Pct Recovery = 96% Analysis Date = 01/07/15 Pct Recovery = 96% Analysis Date = 01/02/15 Pct Recovery = 96% Analysis Date = 01/02/15 Pct Recovery = 96% Analysis Date = 12/28/14 Pct Recovery = 96% Analysis Date = 12/28/14 Pct Recovery = 96% Analysis Date = 12/23/14 Pct Recovery = 96% Analysis Date = 12/23/14 Pct Recovery = 96% Analysis Date = 12/18/14 Pct Recovery = 97% Analysis Date = 12/18/14 Pct Recovery = 97% Analysis Date = 12/14/14 Pct Recovery = 97% Analysis Date = 12/14/14 Pct Recovery = 97% Analysis Date = 12/09/14 Pct Recovery = 97% Analysis Date = 12/09/14 Pct Recovery = 97% Analysis Date = 12/04/14 Pct Recovery = 97% Analysis Date = 12/04/14 Pct Recovery = 97% Analysis Date = 11/29/14 Pct Recovery = 97% Analysis Date = 11/29/14 Pct Recovery = 97% Analysis Date = 11/24/14 Pct Recovery = 98% Analysis Date = 11/24/14 Pct Recovery = 98% Analysis Date = 11/20/14 Pct Recovery = 98% Analysis Date = 11/20/14 Pct Recovery = 98% Analysis Date = 11/15/14 Pct Recovery = 98% Analysis Date = 11/15/14 Pct Recovery = 98% Analysis Date = 11/10/14 Pct Recovery = 98% Analysis Date = 11/10/14 Pct Recovery = 98% Analysis Date = 11/05/14 Pct Recovery = 98% Analysis Date = 11/05/14 Pct Recovery = 98% Analysis Date = 11/01/14 Pct Recovery = 99% Analysis Date = 11/01/14 Pct Recovery = 99% Analysis Date = 10/27/14 Pct Recovery = 99% Analysis Date = 10/27/14 Pct Recovery = 99% Analysis Date = 10/22/14 Pct Recovery = 99% Analysis Date = 10/22/14 Pct Recovery = 99% Analysis Date = 10/17/14 Pct Recovery = 99% Analysis Date = 10/17/14 Pct Recovery = 99% Analysis Date = 10/12/14 Pct Recovery = 100% Analysis Date = 10/12/14 Pct Recovery = 100% Analysis Date = 10/08/14 Pct Recovery = 100% Analysis Date = 10/08/14 Pct Recovery = 100% Analysis Date = 10/03/14 Pct Recovery = 100% Analysis Date = 10/03/14 Pct Recovery = 100% Analysis Date = 09/28/14 Pct Recovery = 100% Analysis Date = 09/28/14 Pct Recovery = 100% Analysis Date = 09/23/14 Pct Recovery = 100% Analysis Date = 09/23/14 Pct Recovery = 100% Analysis Date = 09/18/14 Pct Recovery = 101% Analysis Date = 09/18/14 Pct Recovery = 101% Analysis Date = 09/14/14 Pct Recovery = 101% Analysis Date = 09/14/14 Pct Recovery = 101% Analysis Date = 09/09/14 Pct Recovery = 101% Analysis Date = 09/09/14 Pct Recovery = 101% Analysis Date = 09/04/14 Pct Recovery = 101% Analysis Date = 09/04/14 Pct Recovery = 101% Analysis Date = 08/30/14 Pct Recovery = 102% Analysis Date = 08/30/14 Pct Recovery = 102% Analysis Date = 08/25/14 Pct Recovery = 102% Analysis Date = 08/25/14 Pct Recovery = 102% Analysis Date = 08/21/14 Pct Recovery = 102% Analysis Date = 08/21/14 Pct Recovery = 102% Analysis Date = 08/16/14 Pct Recovery = 102% Analysis Date = 08/16/14 Pct Recovery = 102% Analysis Date = 08/11/14 Pct Recovery = 102% Analysis Date = 08/11/14 Pct Recovery = 102% Analysis Date = 08/06/14 Pct Recovery = 103% Analysis Date = 08/06/14 Pct Recovery = 103% Analysis Date = 08/02/14 Pct Recovery = 103% Analysis Date = 08/02/14 Pct Recovery = 103% Analysis Date = 07/28/14 Pct Recovery = 103% Analysis Date = 07/28/14 Pct Recovery = 103% Analysis Date = 07/23/14 Pct Recovery = 103% Analysis Date = 07/23/14 Pct Recovery = 103% Analysis Date = 07/18/14 Pct Recovery = 103% Analysis Date = 07/18/14 Pct Recovery = 103% Analysis Date = 07/13/14 Pct Recovery = 104% Analysis Date = 07/13/14 Pct Recovery = 104% Analysis Date = 07/09/14 Pct Recovery = 104% Analysis Date = 07/09/14 Pct Recovery = 104% Analysis Date = 07/04/14 Pct Recovery = 104% Analysis Date = 07/04/14 Pct Recovery = 104% Analysis Date = 06/29/14 Pct Recovery = 104% Analysis Date = 06/29/14 Pct Recovery = 104% Analysis Date = 06/24/14 Pct Recovery = 104% Analysis Date = 06/24/14 Pct Recovery = 104% Analysis Date = 06/19/14 Pct Recovery = 105% Analysis Date = 06/19/14 Pct Recovery = 105% Analysis Date = 06/15/14 Pct Recovery = 105% Analysis Date = 06/15/14 Pct Recovery = 105% Analysis Date = 06/10/14 Pct Recovery = 105% Analysis Date = 06/10/14 Pct Recovery = 105% Analysis Date = 06/05/14 Pct Recovery = 105% Analysis Date = 06/05/14 Pct Recovery = 105% Analysis Date = 05/31/14 Pct Recovery = 106% Analysis Date = 05/31/14 Pct Recovery = 106% Analysis Date = 05/26/14 Pct Recovery = 106% Analysis Date = 05/26/14 Pct Recovery = 106% Analysis Date = 05/22/14 Pct Recovery = 106% Analysis Date = 05/22/14 Pct Recovery = 106% Analysis Date = 05/17/14 Pct Recovery = 106% Analysis Date = 05/17/14 Pct Recovery = 106% Analysis Date = 05/12/14 Pct Recovery = 106% Analysis Date = 05/12/14 Pct Recovery = 106% Analysis Date = 05/07/14 Pct Recovery = 107% Analysis Date = 05/07/14 Pct Recovery = 107% Analysis Date = 05/03/14 Pct Recovery = 107% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
TRANS-1,3-DICHLOROPROPENE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 49 96% 13% 95% 14%
Total 49 96% 13% 95% 14%

Sample Statistics
TRANS-1,3-DICHLOROPROPENE

Characteristic N % % Basis
Plotted 49 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 49 .  
False Negatives 0 0% 0 out of 49
Not Spiked 24 .  
False Positives 0 0% 0 out of 24

BQS OBSP Determination:
TRANS-1,4-DICHLORO-2-BUTENE
METHOD: 4440 , TESTIDCODE: 73547GCM66
Open Data Set

Analysis Date = 12/12/16 SpikeMix = Accu 216041125: 40 µl & Crescent 03FF058: 40 µl Pct Recovery = 97% Analysis Date = 07/20/16 SpikeMix = Supelco LC20141V: 40 µl & Accu 216041125: 40 µl Pct Recovery = 102% Analysis Date = 07/14/16 SpikeMix = Accu 216041125: 40 µl & NSI 041816AVOC: 40 µl Pct Recovery = 74% Analysis Date = 08/12/16 SpikeMix = ChemService 5082900: 25 µl & Phenova B20160319: 25 µl Pct Recovery = 73% Analysis Date = 06/21/16 SpikeMix = Phenova B20160319: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 93% Analysis Date = 09/08/16 SpikeMix = Supelco LC20141V: 25 µl & Accu 216041125: 25 µl Pct Recovery = 66% Analysis Date = 05/24/16 SpikeMix = Accu 216041125: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 91% Analysis Date = 03/19/15 SpikeMix = Spex Organics C1140417015: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 108% Analysis Date = 03/06/15 SpikeMix = ERA 0227-14-06.1A: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 56% Analysis Date = 12/17/14 SpikeMix = Supelco LC06438: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 55% Analysis Date = 11/22/14 SpikeMix = NSI 032614: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 90% Analysis Date = 09/21/14 SpikeMix = Supelco LC06438: 20 µl Pct Recovery = 58% Analysis Date = 08/19/14 SpikeMix = Spex Organics C1140417015: 20 µl & Accu 214031115: 20 µl Pct Recovery = 91% Analysis Date = 08/16/14 SpikeMix = ERA 0227-14-06.1A: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 80% Analysis Date = 06/10/14 SpikeMix = NSI 032614: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 70% Analysis Date = 09/29/15 SpikeMix = Accu 215041380: 25 µl & ERA 0406-15-03: 25 µl Pct Recovery = 74% Analysis Date = 08/15/15 SpikeMix = Supelco LC13545: 25 µl & Crescent 04EE008: 25 µl Pct Recovery = 82% Analysis Date = 07/13/15 SpikeMix = Crescent 04EE008: 25 µl & NSI 050515AVOC: 25 µl Pct Recovery = 56% Analysis Date = 11/29/16 SpikeMix = ChemService 5082900: 15 µl & Phenova B20160319: 15 µl Pct Recovery = 79% Analysis Date = 09/08/16 SpikeMix = Phenova B20160319: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 77% Analysis Date = 07/29/16 SpikeMix = Phenova B20160319: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 97% Analysis Date = 05/27/16 SpikeMix = Phenova B20160319: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 85% Analysis Date = 10/13/16 SpikeMix = Accu 216041125: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 80% Analysis Date = 08/20/16 SpikeMix = Accu 216041125: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 86% Analysis Date = 06/30/16 SpikeMix = ChemService 5082900: 15 µl & Accu 216041125: 15 µl Pct Recovery = 54% Analysis Date = 04/02/16 SpikeMix = Supelco LC13545: 15 µl & Accu 215041380: 15 µl Pct Recovery = 83% Analysis Date = 03/04/16 SpikeMix = Accu 215041380: 15 µl & ERA 0406-15-03: 15 µl Pct Recovery = 86% Analysis Date = 06/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Accu 215041380: 15 µl Pct Recovery = 88% Analysis Date = 12/18/15 SpikeMix = Supelco LC13545: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 73% Analysis Date = 10/17/15 SpikeMix = Crescent 04EE008: 15 µl & NSI 050515AVOC: 15 µl Pct Recovery = 75% Analysis Date = 05/09/15 SpikeMix = Spex Organics EN150428007: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 87% Analysis Date = 11/06/14 SpikeMix = Spex Organics C1140417015: 10 µl & Crescent 03DD004: 10 µl Pct Recovery = 98% Analysis Date = 10/21/14 SpikeMix = ERA 0227-14-06.1A: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 58% Analysis Date = 09/09/14 SpikeMix = NSI 032614: 10 µl & Spex Organics C1140417015: 10 µl Pct Recovery = 90% Analysis Date = 07/23/14 SpikeMix = Spex Organics C1140417015: 10 µl & Accu 214031115: 10 µl Pct Recovery = 75% Analysis Date = 07/11/14 SpikeMix = Spex Organics C1140417015: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 73% Analysis Date = 06/18/14 SpikeMix = Supelco LC06438: 10 µl & Accu 214031115: 10 µl Pct Recovery = 70% Analysis Date = 05/30/14 SpikeMix = NSI 032614: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 53% Analysis Date = 05/03/14 SpikeMix = Crescent 03DD004: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 68% Analysis Date = 02/18/16 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 89% Analysis Date = 11/20/15 SpikeMix = Accu 215041380: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 72% Analysis Date = 11/12/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 59% Analysis Date = 05/21/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 89% Analysis Date = 05/13/16 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 75% Analysis Date = 01/27/16 SpikeMix = Crescent 04EE008: 10 µl & NSI 050515AVOC: 10 µl Pct Recovery = 62% Analysis Date = 07/31/15 SpikeMix = Crescent 04EE008: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 72% Analysis Date = 05/09/15 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 82% Analysis Date = 12/12/16 Pct Recovery = 85% Analysis Date = 12/07/16 Pct Recovery = 85% Analysis Date = 12/07/16 Pct Recovery = 85% Analysis Date = 12/02/16 Pct Recovery = 85% Analysis Date = 12/02/16 Pct Recovery = 85% Analysis Date = 11/27/16 Pct Recovery = 85% Analysis Date = 11/27/16 Pct Recovery = 85% Analysis Date = 11/22/16 Pct Recovery = 85% Analysis Date = 11/22/16 Pct Recovery = 85% Analysis Date = 11/18/16 Pct Recovery = 85% Analysis Date = 11/18/16 Pct Recovery = 85% Analysis Date = 11/13/16 Pct Recovery = 84% Analysis Date = 11/13/16 Pct Recovery = 84% Analysis Date = 11/08/16 Pct Recovery = 84% Analysis Date = 11/08/16 Pct Recovery = 84% Analysis Date = 11/03/16 Pct Recovery = 84% Analysis Date = 11/03/16 Pct Recovery = 84% Analysis Date = 10/30/16 Pct Recovery = 84% Analysis Date = 10/30/16 Pct Recovery = 84% Analysis Date = 10/25/16 Pct Recovery = 84% Analysis Date = 10/25/16 Pct Recovery = 84% Analysis Date = 10/20/16 Pct Recovery = 84% Analysis Date = 10/20/16 Pct Recovery = 84% Analysis Date = 10/15/16 Pct Recovery = 84% Analysis Date = 10/15/16 Pct Recovery = 84% Analysis Date = 10/10/16 Pct Recovery = 84% Analysis Date = 10/10/16 Pct Recovery = 84% Analysis Date = 10/06/16 Pct Recovery = 84% Analysis Date = 10/06/16 Pct Recovery = 84% Analysis Date = 10/01/16 Pct Recovery = 83% Analysis Date = 10/01/16 Pct Recovery = 83% Analysis Date = 09/26/16 Pct Recovery = 83% Analysis Date = 09/26/16 Pct Recovery = 83% Analysis Date = 09/21/16 Pct Recovery = 83% Analysis Date = 09/21/16 Pct Recovery = 83% Analysis Date = 09/17/16 Pct Recovery = 83% Analysis Date = 09/17/16 Pct Recovery = 83% Analysis Date = 09/12/16 Pct Recovery = 83% Analysis Date = 09/12/16 Pct Recovery = 83% Analysis Date = 09/07/16 Pct Recovery = 83% Analysis Date = 09/07/16 Pct Recovery = 83% Analysis Date = 09/02/16 Pct Recovery = 83% Analysis Date = 09/02/16 Pct Recovery = 83% Analysis Date = 08/29/16 Pct Recovery = 83% Analysis Date = 08/29/16 Pct Recovery = 83% Analysis Date = 08/24/16 Pct Recovery = 82% Analysis Date = 08/24/16 Pct Recovery = 82% Analysis Date = 08/19/16 Pct Recovery = 82% Analysis Date = 08/19/16 Pct Recovery = 82% Analysis Date = 08/14/16 Pct Recovery = 82% Analysis Date = 08/14/16 Pct Recovery = 82% Analysis Date = 08/09/16 Pct Recovery = 82% Analysis Date = 08/09/16 Pct Recovery = 82% Analysis Date = 08/05/16 Pct Recovery = 82% Analysis Date = 08/05/16 Pct Recovery = 82% Analysis Date = 07/31/16 Pct Recovery = 82% Analysis Date = 07/31/16 Pct Recovery = 82% Analysis Date = 07/26/16 Pct Recovery = 82% Analysis Date = 07/26/16 Pct Recovery = 82% Analysis Date = 07/21/16 Pct Recovery = 82% Analysis Date = 07/21/16 Pct Recovery = 82% Analysis Date = 07/17/16 Pct Recovery = 81% Analysis Date = 07/17/16 Pct Recovery = 81% Analysis Date = 07/12/16 Pct Recovery = 81% Analysis Date = 07/12/16 Pct Recovery = 81% Analysis Date = 07/07/16 Pct Recovery = 81% Analysis Date = 07/07/16 Pct Recovery = 81% Analysis Date = 07/02/16 Pct Recovery = 81% Analysis Date = 07/02/16 Pct Recovery = 81% Analysis Date = 06/28/16 Pct Recovery = 81% Analysis Date = 06/28/16 Pct Recovery = 81% Analysis Date = 06/23/16 Pct Recovery = 81% Analysis Date = 06/23/16 Pct Recovery = 81% Analysis Date = 06/18/16 Pct Recovery = 81% Analysis Date = 06/18/16 Pct Recovery = 81% Analysis Date = 06/13/16 Pct Recovery = 80% Analysis Date = 06/13/16 Pct Recovery = 80% Analysis Date = 06/08/16 Pct Recovery = 80% Analysis Date = 06/08/16 Pct Recovery = 80% Analysis Date = 06/04/16 Pct Recovery = 80% Analysis Date = 06/04/16 Pct Recovery = 80% Analysis Date = 05/30/16 Pct Recovery = 80% Analysis Date = 05/30/16 Pct Recovery = 80% Analysis Date = 05/25/16 Pct Recovery = 80% Analysis Date = 05/25/16 Pct Recovery = 80% Analysis Date = 05/20/16 Pct Recovery = 80% Analysis Date = 05/20/16 Pct Recovery = 80% Analysis Date = 05/16/16 Pct Recovery = 80% Analysis Date = 05/16/16 Pct Recovery = 80% Analysis Date = 05/11/16 Pct Recovery = 79% Analysis Date = 05/11/16 Pct Recovery = 79% Analysis Date = 05/06/16 Pct Recovery = 79% Analysis Date = 05/06/16 Pct Recovery = 79% Analysis Date = 05/01/16 Pct Recovery = 79% Analysis Date = 05/01/16 Pct Recovery = 79% Analysis Date = 04/27/16 Pct Recovery = 79% Analysis Date = 04/27/16 Pct Recovery = 79% Analysis Date = 04/22/16 Pct Recovery = 79% Analysis Date = 04/22/16 Pct Recovery = 79% Analysis Date = 04/17/16 Pct Recovery = 79% Analysis Date = 04/17/16 Pct Recovery = 79% Analysis Date = 04/12/16 Pct Recovery = 79% Analysis Date = 04/12/16 Pct Recovery = 79% Analysis Date = 04/07/16 Pct Recovery = 79% Analysis Date = 04/07/16 Pct Recovery = 79% Analysis Date = 04/03/16 Pct Recovery = 78% Analysis Date = 04/03/16 Pct Recovery = 78% Analysis Date = 03/29/16 Pct Recovery = 78% Analysis Date = 03/29/16 Pct Recovery = 78% Analysis Date = 03/24/16 Pct Recovery = 78% Analysis Date = 03/24/16 Pct Recovery = 78% Analysis Date = 03/19/16 Pct Recovery = 78% Analysis Date = 03/19/16 Pct Recovery = 78% Analysis Date = 03/15/16 Pct Recovery = 78% Analysis Date = 03/15/16 Pct Recovery = 78% Analysis Date = 03/10/16 Pct Recovery = 78% Analysis Date = 03/10/16 Pct Recovery = 78% Analysis Date = 03/05/16 Pct Recovery = 78% Analysis Date = 03/05/16 Pct Recovery = 78% Analysis Date = 02/29/16 Pct Recovery = 77% Analysis Date = 02/29/16 Pct Recovery = 77% Analysis Date = 02/25/16 Pct Recovery = 77% Analysis Date = 02/25/16 Pct Recovery = 77% Analysis Date = 02/20/16 Pct Recovery = 77% Analysis Date = 02/20/16 Pct Recovery = 77% Analysis Date = 02/15/16 Pct Recovery = 77% Analysis Date = 02/15/16 Pct Recovery = 77% Analysis Date = 02/10/16 Pct Recovery = 77% Analysis Date = 02/10/16 Pct Recovery = 77% Analysis Date = 02/05/16 Pct Recovery = 77% Analysis Date = 02/05/16 Pct Recovery = 77% Analysis Date = 02/01/16 Pct Recovery = 77% Analysis Date = 02/01/16 Pct Recovery = 77% Analysis Date = 01/27/16 Pct Recovery = 77% Analysis Date = 01/27/16 Pct Recovery = 77% Analysis Date = 01/22/16 Pct Recovery = 77% Analysis Date = 01/22/16 Pct Recovery = 77% Analysis Date = 01/17/16 Pct Recovery = 77% Analysis Date = 01/17/16 Pct Recovery = 77% Analysis Date = 01/13/16 Pct Recovery = 77% Analysis Date = 01/13/16 Pct Recovery = 77% Analysis Date = 01/08/16 Pct Recovery = 77% Analysis Date = 01/08/16 Pct Recovery = 77% Analysis Date = 01/03/16 Pct Recovery = 76% Analysis Date = 01/03/16 Pct Recovery = 76% Analysis Date = 12/29/15 Pct Recovery = 76% Analysis Date = 12/29/15 Pct Recovery = 76% Analysis Date = 12/25/15 Pct Recovery = 76% Analysis Date = 12/25/15 Pct Recovery = 76% Analysis Date = 12/20/15 Pct Recovery = 76% Analysis Date = 12/20/15 Pct Recovery = 76% Analysis Date = 12/15/15 Pct Recovery = 76% Analysis Date = 12/15/15 Pct Recovery = 76% Analysis Date = 12/10/15 Pct Recovery = 76% Analysis Date = 12/10/15 Pct Recovery = 76% Analysis Date = 12/05/15 Pct Recovery = 76% Analysis Date = 12/05/15 Pct Recovery = 76% Analysis Date = 12/01/15 Pct Recovery = 76% Analysis Date = 12/01/15 Pct Recovery = 76% Analysis Date = 11/26/15 Pct Recovery = 76% Analysis Date = 11/26/15 Pct Recovery = 76% Analysis Date = 11/21/15 Pct Recovery = 76% Analysis Date = 11/21/15 Pct Recovery = 76% Analysis Date = 11/16/15 Pct Recovery = 76% Analysis Date = 11/16/15 Pct Recovery = 76% Analysis Date = 11/12/15 Pct Recovery = 76% Analysis Date = 11/12/15 Pct Recovery = 76% Analysis Date = 11/07/15 Pct Recovery = 76% Analysis Date = 11/07/15 Pct Recovery = 76% Analysis Date = 11/02/15 Pct Recovery = 76% Analysis Date = 11/02/15 Pct Recovery = 76% Analysis Date = 10/28/15 Pct Recovery = 76% Analysis Date = 10/28/15 Pct Recovery = 76% Analysis Date = 10/24/15 Pct Recovery = 76% Analysis Date = 10/24/15 Pct Recovery = 76% Analysis Date = 10/19/15 Pct Recovery = 76% Analysis Date = 10/19/15 Pct Recovery = 76% Analysis Date = 10/14/15 Pct Recovery = 76% Analysis Date = 10/14/15 Pct Recovery = 76% Analysis Date = 10/09/15 Pct Recovery = 76% Analysis Date = 10/09/15 Pct Recovery = 76% Analysis Date = 10/04/15 Pct Recovery = 76% Analysis Date = 10/04/15 Pct Recovery = 76% Analysis Date = 09/30/15 Pct Recovery = 77% Analysis Date = 09/30/15 Pct Recovery = 77% Analysis Date = 09/25/15 Pct Recovery = 77% Analysis Date = 09/25/15 Pct Recovery = 77% Analysis Date = 09/20/15 Pct Recovery = 77% Analysis Date = 09/20/15 Pct Recovery = 77% Analysis Date = 09/15/15 Pct Recovery = 77% Analysis Date = 09/15/15 Pct Recovery = 77% Analysis Date = 09/11/15 Pct Recovery = 77% Analysis Date = 09/11/15 Pct Recovery = 77% Analysis Date = 09/06/15 Pct Recovery = 77% Analysis Date = 09/06/15 Pct Recovery = 77% Analysis Date = 09/01/15 Pct Recovery = 77% Analysis Date = 09/01/15 Pct Recovery = 77% Analysis Date = 08/27/15 Pct Recovery = 77% Analysis Date = 08/27/15 Pct Recovery = 77% Analysis Date = 08/23/15 Pct Recovery = 77% Analysis Date = 08/23/15 Pct Recovery = 77% Analysis Date = 08/18/15 Pct Recovery = 77% Analysis Date = 08/18/15 Pct Recovery = 77% Analysis Date = 08/13/15 Pct Recovery = 77% Analysis Date = 08/13/15 Pct Recovery = 77% Analysis Date = 08/08/15 Pct Recovery = 77% Analysis Date = 08/08/15 Pct Recovery = 77% Analysis Date = 08/03/15 Pct Recovery = 77% Analysis Date = 08/03/15 Pct Recovery = 77% Analysis Date = 07/30/15 Pct Recovery = 77% Analysis Date = 07/30/15 Pct Recovery = 77% Analysis Date = 07/25/15 Pct Recovery = 77% Analysis Date = 07/25/15 Pct Recovery = 77% Analysis Date = 07/20/15 Pct Recovery = 77% Analysis Date = 07/20/15 Pct Recovery = 77% Analysis Date = 07/15/15 Pct Recovery = 77% Analysis Date = 07/15/15 Pct Recovery = 77% Analysis Date = 07/11/15 Pct Recovery = 77% Analysis Date = 07/11/15 Pct Recovery = 77% Analysis Date = 07/06/15 Pct Recovery = 77% Analysis Date = 07/06/15 Pct Recovery = 77% Analysis Date = 07/01/15 Pct Recovery = 77% Analysis Date = 07/01/15 Pct Recovery = 77% Analysis Date = 06/26/15 Pct Recovery = 77% Analysis Date = 06/26/15 Pct Recovery = 77% Analysis Date = 06/21/15 Pct Recovery = 77% Analysis Date = 06/21/15 Pct Recovery = 77% Analysis Date = 06/17/15 Pct Recovery = 77% Analysis Date = 06/17/15 Pct Recovery = 77% Analysis Date = 06/12/15 Pct Recovery = 77% Analysis Date = 06/12/15 Pct Recovery = 77% Analysis Date = 06/07/15 Pct Recovery = 77% Analysis Date = 06/07/15 Pct Recovery = 77% Analysis Date = 06/02/15 Pct Recovery = 77% Analysis Date = 06/02/15 Pct Recovery = 77% Analysis Date = 05/29/15 Pct Recovery = 77% Analysis Date = 05/29/15 Pct Recovery = 77% Analysis Date = 05/24/15 Pct Recovery = 77% Analysis Date = 05/24/15 Pct Recovery = 77% Analysis Date = 05/19/15 Pct Recovery = 77% Analysis Date = 05/19/15 Pct Recovery = 77% Analysis Date = 05/14/15 Pct Recovery = 77% Analysis Date = 05/14/15 Pct Recovery = 77% Analysis Date = 05/10/15 Pct Recovery = 77% Analysis Date = 05/10/15 Pct Recovery = 77% Analysis Date = 05/05/15 Pct Recovery = 77% Analysis Date = 05/05/15 Pct Recovery = 77% Analysis Date = 04/30/15 Pct Recovery = 77% Analysis Date = 04/30/15 Pct Recovery = 77% Analysis Date = 04/25/15 Pct Recovery = 78% Analysis Date = 04/25/15 Pct Recovery = 78% Analysis Date = 04/20/15 Pct Recovery = 78% Analysis Date = 04/20/15 Pct Recovery = 78% Analysis Date = 04/16/15 Pct Recovery = 78% Analysis Date = 04/16/15 Pct Recovery = 78% Analysis Date = 04/11/15 Pct Recovery = 78% Analysis Date = 04/11/15 Pct Recovery = 78% Analysis Date = 04/06/15 Pct Recovery = 78% Analysis Date = 04/06/15 Pct Recovery = 78% Analysis Date = 04/01/15 Pct Recovery = 78% Analysis Date = 04/01/15 Pct Recovery = 78% Analysis Date = 03/28/15 Pct Recovery = 78% Analysis Date = 03/28/15 Pct Recovery = 78% Analysis Date = 03/23/15 Pct Recovery = 78% Analysis Date = 03/23/15 Pct Recovery = 78% Analysis Date = 03/18/15 Pct Recovery = 78% Analysis Date = 03/18/15 Pct Recovery = 78% Analysis Date = 03/13/15 Pct Recovery = 78% Analysis Date = 03/13/15 Pct Recovery = 78% Analysis Date = 03/09/15 Pct Recovery = 78% Analysis Date = 03/09/15 Pct Recovery = 78% Analysis Date = 03/04/15 Pct Recovery = 78% Analysis Date = 03/04/15 Pct Recovery = 78% Analysis Date = 02/27/15 Pct Recovery = 78% Analysis Date = 02/27/15 Pct Recovery = 78% Analysis Date = 02/22/15 Pct Recovery = 78% Analysis Date = 02/22/15 Pct Recovery = 78% Analysis Date = 02/17/15 Pct Recovery = 78% Analysis Date = 02/17/15 Pct Recovery = 78% Analysis Date = 02/13/15 Pct Recovery = 78% Analysis Date = 02/13/15 Pct Recovery = 78% Analysis Date = 02/08/15 Pct Recovery = 78% Analysis Date = 02/08/15 Pct Recovery = 78% Analysis Date = 02/03/15 Pct Recovery = 78% Analysis Date = 02/03/15 Pct Recovery = 78% Analysis Date = 01/29/15 Pct Recovery = 78% Analysis Date = 01/29/15 Pct Recovery = 78% Analysis Date = 01/25/15 Pct Recovery = 77% Analysis Date = 01/25/15 Pct Recovery = 77% Analysis Date = 01/20/15 Pct Recovery = 77% Analysis Date = 01/20/15 Pct Recovery = 77% Analysis Date = 01/15/15 Pct Recovery = 77% Analysis Date = 01/15/15 Pct Recovery = 77% Analysis Date = 01/10/15 Pct Recovery = 77% Analysis Date = 01/10/15 Pct Recovery = 77% Analysis Date = 01/06/15 Pct Recovery = 77% Analysis Date = 01/06/15 Pct Recovery = 77% Analysis Date = 01/01/15 Pct Recovery = 77% Analysis Date = 01/01/15 Pct Recovery = 77% Analysis Date = 12/27/14 Pct Recovery = 77% Analysis Date = 12/27/14 Pct Recovery = 77% Analysis Date = 12/22/14 Pct Recovery = 77% Analysis Date = 12/22/14 Pct Recovery = 77% Analysis Date = 12/17/14 Pct Recovery = 77% Analysis Date = 12/17/14 Pct Recovery = 77% Analysis Date = 12/13/14 Pct Recovery = 77% Analysis Date = 12/13/14 Pct Recovery = 77% Analysis Date = 12/08/14 Pct Recovery = 76% Analysis Date = 12/08/14 Pct Recovery = 76% Analysis Date = 12/03/14 Pct Recovery = 76% Analysis Date = 12/03/14 Pct Recovery = 76% Analysis Date = 11/28/14 Pct Recovery = 76% Analysis Date = 11/28/14 Pct Recovery = 76% Analysis Date = 11/24/14 Pct Recovery = 76% Analysis Date = 11/24/14 Pct Recovery = 76% Analysis Date = 11/19/14 Pct Recovery = 76% Analysis Date = 11/19/14 Pct Recovery = 76% Analysis Date = 11/14/14 Pct Recovery = 76% Analysis Date = 11/14/14 Pct Recovery = 76% Analysis Date = 11/09/14 Pct Recovery = 76% Analysis Date = 11/09/14 Pct Recovery = 76% Analysis Date = 11/05/14 Pct Recovery = 76% Analysis Date = 11/05/14 Pct Recovery = 76% Analysis Date = 10/31/14 Pct Recovery = 76% Analysis Date = 10/31/14 Pct Recovery = 76% Analysis Date = 10/26/14 Pct Recovery = 75% Analysis Date = 10/26/14 Pct Recovery = 75% Analysis Date = 10/21/14 Pct Recovery = 75% Analysis Date = 10/21/14 Pct Recovery = 75% Analysis Date = 10/16/14 Pct Recovery = 75% Analysis Date = 10/16/14 Pct Recovery = 75% Analysis Date = 10/12/14 Pct Recovery = 75% Analysis Date = 10/12/14 Pct Recovery = 75% Analysis Date = 10/07/14 Pct Recovery = 75% Analysis Date = 10/07/14 Pct Recovery = 75% Analysis Date = 10/02/14 Pct Recovery = 75% Analysis Date = 10/02/14 Pct Recovery = 75% Analysis Date = 09/27/14 Pct Recovery = 75% Analysis Date = 09/27/14 Pct Recovery = 75% Analysis Date = 09/23/14 Pct Recovery = 74% Analysis Date = 09/23/14 Pct Recovery = 74% Analysis Date = 09/18/14 Pct Recovery = 74% Analysis Date = 09/18/14 Pct Recovery = 74% Analysis Date = 09/13/14 Pct Recovery = 74% Analysis Date = 09/13/14 Pct Recovery = 74% Analysis Date = 09/08/14 Pct Recovery = 74% Analysis Date = 09/08/14 Pct Recovery = 74% Analysis Date = 09/04/14 Pct Recovery = 74% Analysis Date = 09/04/14 Pct Recovery = 74% Analysis Date = 08/30/14 Pct Recovery = 74% Analysis Date = 08/30/14 Pct Recovery = 74% Analysis Date = 08/25/14 Pct Recovery = 74% Analysis Date = 08/25/14 Pct Recovery = 74% Analysis Date = 08/20/14 Pct Recovery = 73% Analysis Date = 08/20/14 Pct Recovery = 73% Analysis Date = 08/15/14 Pct Recovery = 73% Analysis Date = 08/15/14 Pct Recovery = 73% Analysis Date = 08/11/14 Pct Recovery = 73% Analysis Date = 08/11/14 Pct Recovery = 73% Analysis Date = 08/06/14 Pct Recovery = 73% Analysis Date = 08/06/14 Pct Recovery = 73% Analysis Date = 08/01/14 Pct Recovery = 73% Analysis Date = 08/01/14 Pct Recovery = 73% Analysis Date = 07/27/14 Pct Recovery = 73% Analysis Date = 07/27/14 Pct Recovery = 73% Analysis Date = 07/23/14 Pct Recovery = 72% Analysis Date = 07/23/14 Pct Recovery = 72% Analysis Date = 07/18/14 Pct Recovery = 72% Analysis Date = 07/18/14 Pct Recovery = 72% Analysis Date = 07/13/14 Pct Recovery = 72% Analysis Date = 07/13/14 Pct Recovery = 72% Analysis Date = 07/08/14 Pct Recovery = 72% Analysis Date = 07/08/14 Pct Recovery = 72% Analysis Date = 07/04/14 Pct Recovery = 72% Analysis Date = 07/04/14 Pct Recovery = 72% Analysis Date = 06/29/14 Pct Recovery = 72% Analysis Date = 06/29/14 Pct Recovery = 72% Analysis Date = 06/24/14 Pct Recovery = 71% Analysis Date = 06/24/14 Pct Recovery = 71% Analysis Date = 06/19/14 Pct Recovery = 71% Analysis Date = 06/19/14 Pct Recovery = 71% Analysis Date = 06/14/14 Pct Recovery = 71% Analysis Date = 06/14/14 Pct Recovery = 71% Analysis Date = 06/10/14 Pct Recovery = 71% Analysis Date = 06/10/14 Pct Recovery = 71% Analysis Date = 06/05/14 Pct Recovery = 71% Analysis Date = 06/05/14 Pct Recovery = 71% Analysis Date = 05/31/14 Pct Recovery = 71% Analysis Date = 05/31/14 Pct Recovery = 71% Analysis Date = 05/26/14 Pct Recovery = 71% Analysis Date = 05/26/14 Pct Recovery = 71% Analysis Date = 05/22/14 Pct Recovery = 70% Analysis Date = 05/22/14 Pct Recovery = 70% Analysis Date = 05/17/14 Pct Recovery = 70% Analysis Date = 05/17/14 Pct Recovery = 70% Analysis Date = 05/12/14 Pct Recovery = 70% Analysis Date = 05/12/14 Pct Recovery = 70% Analysis Date = 05/07/14 Pct Recovery = 70% Analysis Date = 05/07/14 Pct Recovery = 70% Analysis Date = 05/03/14 Pct Recovery = 70% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
TRANS-1,4-DICHLORO-2-BUTENE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 47 78% 14% 77% 14%
Total 47 78% 14% 77% 14%

Sample Statistics
TRANS-1,4-DICHLORO-2-BUTENE

Characteristic N % % Basis
Plotted 47 100% Spiked
Estimated Values 47 100% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 47 .  
False Negatives 0 0% 0 out of 47
Not Spiked 26 .  
False Positives 0 0% 0 out of 26

BQS OBSP Determination:
TRICHLOROETHYLENE
METHOD: 4440 , TESTIDCODE: 39180GCM66
Open Data Set

Analysis Date = 12/12/16 SpikeMix = Accu 216041125: 40 µl & Crescent 03FF058: 40 µl Pct Recovery = 101% Analysis Date = 07/20/16 SpikeMix = Supelco LC20141V: 40 µl & Accu 216041125: 40 µl Pct Recovery = 110% Analysis Date = 07/14/16 SpikeMix = Accu 216041125: 40 µl & NSI 041816AVOC: 40 µl Pct Recovery = 121% Analysis Date = 08/12/16 SpikeMix = ChemService 5082900: 25 µl & Phenova B20160319: 25 µl Pct Recovery = 90% Analysis Date = 06/21/16 SpikeMix = Phenova B20160319: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 94% Analysis Date = 09/08/16 SpikeMix = Supelco LC20141V: 25 µl & Accu 216041125: 25 µl Pct Recovery = 88% Analysis Date = 05/24/16 SpikeMix = Accu 216041125: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 90% Analysis Date = 04/09/15 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 101% Analysis Date = 03/06/15 SpikeMix = ERA 0227-14-06.1A: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 87% Analysis Date = 11/14/14 SpikeMix = Crescent 03DD004: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 94% Analysis Date = 08/16/14 SpikeMix = ERA 0227-14-06.1A: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 93% Analysis Date = 07/01/14 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 104% Analysis Date = 11/22/14 SpikeMix = NSI 032614: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 94% Analysis Date = 06/10/14 SpikeMix = Crescent 03DD004: 20 µl & NSI 032614: 20 µl Pct Recovery = 119% Analysis Date = 06/10/14 SpikeMix = NSI 032614: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 130% Analysis Date = 05/01/14 SpikeMix = Accu 214031115: 20 µl & NSI 032614: 20 µl Pct Recovery = 90% Analysis Date = 07/13/15 SpikeMix = Crescent 04EE008: 25 µl & NSI 050515AVOC: 25 µl Pct Recovery = 114% Analysis Date = 09/29/15 SpikeMix = Accu 215041380: 25 µl & ERA 0406-15-03: 25 µl Pct Recovery = 100% Analysis Date = 06/16/15 SpikeMix = ERA 0406-15-03: 25 µl & Supelco LC13545: 25 µl Pct Recovery = 104% Analysis Date = 11/29/16 SpikeMix = ChemService 5082900: 15 µl & Phenova B20160319: 15 µl Pct Recovery = 103% Analysis Date = 09/08/16 SpikeMix = Phenova B20160319: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 95% Analysis Date = 07/29/16 SpikeMix = Phenova B20160319: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 128% Analysis Date = 05/27/16 SpikeMix = Phenova B20160319: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 104% Analysis Date = 10/13/16 SpikeMix = Accu 216041125: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 148% Analysis Date = 08/20/16 SpikeMix = Accu 216041125: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 101% Analysis Date = 06/30/16 SpikeMix = ChemService 5082900: 15 µl & Accu 216041125: 15 µl Pct Recovery = 66% Analysis Date = 11/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 114% Analysis Date = 10/17/15 SpikeMix = Crescent 04EE008: 15 µl & NSI 050515AVOC: 15 µl Pct Recovery = 111% Analysis Date = 06/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Accu 215041380: 15 µl Pct Recovery = 119% Analysis Date = 04/26/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 100% Analysis Date = 03/04/16 SpikeMix = Accu 215041380: 15 µl & ERA 0406-15-03: 15 µl Pct Recovery = 108% Analysis Date = 02/05/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 98% Analysis Date = 10/16/15 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 105% Analysis Date = 01/13/15 SpikeMix = Accu 214031115: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 113% Analysis Date = 10/21/14 SpikeMix = ERA 0227-14-06.1A: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 97% Analysis Date = 10/04/14 SpikeMix = Crescent 03DD004: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 95% Analysis Date = 07/11/14 SpikeMix = Spex Organics C1140417015: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 98% Analysis Date = 09/09/14 SpikeMix = Accu 214031115: 10 µl & NSI 032614: 10 µl Pct Recovery = 150% Analysis Date = 09/09/14 SpikeMix = NSI 032614: 10 µl & Spex Organics C1140417015: 10 µl Pct Recovery = 112% Analysis Date = 07/29/14 SpikeMix = Crescent 03DD004: 10 µl & NSI 032614: 10 µl Pct Recovery = 91% Analysis Date = 05/30/14 SpikeMix = NSI 032614: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 154% Analysis Date = 03/17/16 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 143% Analysis Date = 01/27/16 SpikeMix = Crescent 04EE008: 10 µl & NSI 050515AVOC: 10 µl Pct Recovery = 119% Analysis Date = 12/10/15 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 128% Analysis Date = 09/03/15 SpikeMix = NSI 050515AVOC: 10 µl & Spex Organics EN150428007: 10 µl Pct Recovery = 120% Analysis Date = 11/20/15 SpikeMix = Accu 215041380: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 106% Analysis Date = 07/31/15 SpikeMix = Crescent 04EE008: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 98% Analysis Date = 06/27/15 SpikeMix = ERA 0406-15-03: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 95% Analysis Date = 12/11/16 Pct Recovery = 103% Analysis Date = 12/07/16 Pct Recovery = 103% Analysis Date = 12/07/16 Pct Recovery = 103% Analysis Date = 12/02/16 Pct Recovery = 104% Analysis Date = 12/02/16 Pct Recovery = 104% Analysis Date = 11/27/16 Pct Recovery = 104% Analysis Date = 11/27/16 Pct Recovery = 104% Analysis Date = 11/22/16 Pct Recovery = 104% Analysis Date = 11/22/16 Pct Recovery = 104% Analysis Date = 11/18/16 Pct Recovery = 104% Analysis Date = 11/18/16 Pct Recovery = 104% Analysis Date = 11/13/16 Pct Recovery = 104% Analysis Date = 11/13/16 Pct Recovery = 104% Analysis Date = 11/08/16 Pct Recovery = 104% Analysis Date = 11/08/16 Pct Recovery = 104% Analysis Date = 11/03/16 Pct Recovery = 104% Analysis Date = 11/03/16 Pct Recovery = 104% Analysis Date = 10/29/16 Pct Recovery = 104% Analysis Date = 10/29/16 Pct Recovery = 104% Analysis Date = 10/25/16 Pct Recovery = 104% Analysis Date = 10/25/16 Pct Recovery = 104% Analysis Date = 10/20/16 Pct Recovery = 104% Analysis Date = 10/20/16 Pct Recovery = 104% Analysis Date = 10/15/16 Pct Recovery = 104% Analysis Date = 10/15/16 Pct Recovery = 104% Analysis Date = 10/10/16 Pct Recovery = 104% Analysis Date = 10/10/16 Pct Recovery = 104% Analysis Date = 10/06/16 Pct Recovery = 104% Analysis Date = 10/06/16 Pct Recovery = 104% Analysis Date = 10/01/16 Pct Recovery = 104% Analysis Date = 10/01/16 Pct Recovery = 104% Analysis Date = 09/26/16 Pct Recovery = 104% Analysis Date = 09/26/16 Pct Recovery = 104% Analysis Date = 09/21/16 Pct Recovery = 104% Analysis Date = 09/21/16 Pct Recovery = 104% Analysis Date = 09/16/16 Pct Recovery = 104% Analysis Date = 09/16/16 Pct Recovery = 104% Analysis Date = 09/12/16 Pct Recovery = 104% Analysis Date = 09/12/16 Pct Recovery = 104% Analysis Date = 09/07/16 Pct Recovery = 104% Analysis Date = 09/07/16 Pct Recovery = 104% Analysis Date = 09/02/16 Pct Recovery = 105% Analysis Date = 09/02/16 Pct Recovery = 105% Analysis Date = 08/28/16 Pct Recovery = 105% Analysis Date = 08/28/16 Pct Recovery = 105% Analysis Date = 08/24/16 Pct Recovery = 105% Analysis Date = 08/24/16 Pct Recovery = 105% Analysis Date = 08/19/16 Pct Recovery = 105% Analysis Date = 08/19/16 Pct Recovery = 105% Analysis Date = 08/14/16 Pct Recovery = 105% Analysis Date = 08/14/16 Pct Recovery = 105% Analysis Date = 08/09/16 Pct Recovery = 105% Analysis Date = 08/09/16 Pct Recovery = 105% Analysis Date = 08/04/16 Pct Recovery = 105% Analysis Date = 08/04/16 Pct Recovery = 105% Analysis Date = 07/31/16 Pct Recovery = 105% Analysis Date = 07/31/16 Pct Recovery = 105% Analysis Date = 07/26/16 Pct Recovery = 105% Analysis Date = 07/26/16 Pct Recovery = 105% Analysis Date = 07/21/16 Pct Recovery = 105% Analysis Date = 07/21/16 Pct Recovery = 105% Analysis Date = 07/16/16 Pct Recovery = 105% Analysis Date = 07/16/16 Pct Recovery = 105% Analysis Date = 07/12/16 Pct Recovery = 106% Analysis Date = 07/12/16 Pct Recovery = 106% Analysis Date = 07/07/16 Pct Recovery = 106% Analysis Date = 07/07/16 Pct Recovery = 106% Analysis Date = 07/02/16 Pct Recovery = 106% Analysis Date = 07/02/16 Pct Recovery = 106% Analysis Date = 06/27/16 Pct Recovery = 106% Analysis Date = 06/27/16 Pct Recovery = 106% Analysis Date = 06/22/16 Pct Recovery = 106% Analysis Date = 06/22/16 Pct Recovery = 106% Analysis Date = 06/18/16 Pct Recovery = 106% Analysis Date = 06/18/16 Pct Recovery = 106% Analysis Date = 06/13/16 Pct Recovery = 106% Analysis Date = 06/13/16 Pct Recovery = 106% Analysis Date = 06/08/16 Pct Recovery = 106% Analysis Date = 06/08/16 Pct Recovery = 106% Analysis Date = 06/03/16 Pct Recovery = 106% Analysis Date = 06/03/16 Pct Recovery = 106% Analysis Date = 05/30/16 Pct Recovery = 106% Analysis Date = 05/30/16 Pct Recovery = 106% Analysis Date = 05/25/16 Pct Recovery = 106% Analysis Date = 05/25/16 Pct Recovery = 106% Analysis Date = 05/20/16 Pct Recovery = 107% Analysis Date = 05/20/16 Pct Recovery = 107% Analysis Date = 05/15/16 Pct Recovery = 107% Analysis Date = 05/15/16 Pct Recovery = 107% Analysis Date = 05/10/16 Pct Recovery = 107% Analysis Date = 05/10/16 Pct Recovery = 107% Analysis Date = 05/06/16 Pct Recovery = 107% Analysis Date = 05/06/16 Pct Recovery = 107% Analysis Date = 05/01/16 Pct Recovery = 107% Analysis Date = 05/01/16 Pct Recovery = 107% Analysis Date = 04/26/16 Pct Recovery = 107% Analysis Date = 04/26/16 Pct Recovery = 107% Analysis Date = 04/21/16 Pct Recovery = 107% Analysis Date = 04/21/16 Pct Recovery = 107% Analysis Date = 04/16/16 Pct Recovery = 107% Analysis Date = 04/16/16 Pct Recovery = 107% Analysis Date = 04/12/16 Pct Recovery = 107% Analysis Date = 04/12/16 Pct Recovery = 107% Analysis Date = 04/07/16 Pct Recovery = 107% Analysis Date = 04/07/16 Pct Recovery = 107% Analysis Date = 04/02/16 Pct Recovery = 107% Analysis Date = 04/02/16 Pct Recovery = 107% Analysis Date = 03/28/16 Pct Recovery = 107% Analysis Date = 03/28/16 Pct Recovery = 107% Analysis Date = 03/24/16 Pct Recovery = 108% Analysis Date = 03/24/16 Pct Recovery = 108% Analysis Date = 03/19/16 Pct Recovery = 108% Analysis Date = 03/19/16 Pct Recovery = 108% Analysis Date = 03/14/16 Pct Recovery = 108% Analysis Date = 03/14/16 Pct Recovery = 108% Analysis Date = 03/09/16 Pct Recovery = 108% Analysis Date = 03/09/16 Pct Recovery = 108% Analysis Date = 03/04/16 Pct Recovery = 108% Analysis Date = 03/04/16 Pct Recovery = 108% Analysis Date = 02/29/16 Pct Recovery = 108% Analysis Date = 02/29/16 Pct Recovery = 108% Analysis Date = 02/24/16 Pct Recovery = 108% Analysis Date = 02/24/16 Pct Recovery = 108% Analysis Date = 02/19/16 Pct Recovery = 109% Analysis Date = 02/19/16 Pct Recovery = 109% Analysis Date = 02/14/16 Pct Recovery = 109% Analysis Date = 02/14/16 Pct Recovery = 109% Analysis Date = 02/10/16 Pct Recovery = 109% Analysis Date = 02/10/16 Pct Recovery = 109% Analysis Date = 02/05/16 Pct Recovery = 109% Analysis Date = 02/05/16 Pct Recovery = 109% Analysis Date = 01/31/16 Pct Recovery = 109% Analysis Date = 01/31/16 Pct Recovery = 109% Analysis Date = 01/26/16 Pct Recovery = 109% Analysis Date = 01/26/16 Pct Recovery = 109% Analysis Date = 01/21/16 Pct Recovery = 109% Analysis Date = 01/21/16 Pct Recovery = 109% Analysis Date = 01/17/16 Pct Recovery = 109% Analysis Date = 01/17/16 Pct Recovery = 109% Analysis Date = 01/12/16 Pct Recovery = 109% Analysis Date = 01/12/16 Pct Recovery = 109% Analysis Date = 01/07/16 Pct Recovery = 110% Analysis Date = 01/07/16 Pct Recovery = 110% Analysis Date = 01/02/16 Pct Recovery = 110% Analysis Date = 01/02/16 Pct Recovery = 110% Analysis Date = 12/29/15 Pct Recovery = 110% Analysis Date = 12/29/15 Pct Recovery = 110% Analysis Date = 12/24/15 Pct Recovery = 110% Analysis Date = 12/24/15 Pct Recovery = 110% Analysis Date = 12/19/15 Pct Recovery = 110% Analysis Date = 12/19/15 Pct Recovery = 110% Analysis Date = 12/14/15 Pct Recovery = 110% Analysis Date = 12/14/15 Pct Recovery = 110% Analysis Date = 12/09/15 Pct Recovery = 110% Analysis Date = 12/09/15 Pct Recovery = 110% Analysis Date = 12/05/15 Pct Recovery = 110% Analysis Date = 12/05/15 Pct Recovery = 110% Analysis Date = 11/30/15 Pct Recovery = 110% Analysis Date = 11/30/15 Pct Recovery = 110% Analysis Date = 11/25/15 Pct Recovery = 110% Analysis Date = 11/25/15 Pct Recovery = 110% Analysis Date = 11/20/15 Pct Recovery = 110% Analysis Date = 11/20/15 Pct Recovery = 110% Analysis Date = 11/16/15 Pct Recovery = 110% Analysis Date = 11/16/15 Pct Recovery = 110% Analysis Date = 11/11/15 Pct Recovery = 110% Analysis Date = 11/11/15 Pct Recovery = 110% Analysis Date = 11/06/15 Pct Recovery = 110% Analysis Date = 11/06/15 Pct Recovery = 110% Analysis Date = 11/01/15 Pct Recovery = 110% Analysis Date = 11/01/15 Pct Recovery = 110% Analysis Date = 10/27/15 Pct Recovery = 110% Analysis Date = 10/27/15 Pct Recovery = 110% Analysis Date = 10/23/15 Pct Recovery = 109% Analysis Date = 10/23/15 Pct Recovery = 109% Analysis Date = 10/18/15 Pct Recovery = 109% Analysis Date = 10/18/15 Pct Recovery = 109% Analysis Date = 10/13/15 Pct Recovery = 109% Analysis Date = 10/13/15 Pct Recovery = 109% Analysis Date = 10/08/15 Pct Recovery = 109% Analysis Date = 10/08/15 Pct Recovery = 109% Analysis Date = 10/04/15 Pct Recovery = 109% Analysis Date = 10/04/15 Pct Recovery = 109% Analysis Date = 09/29/15 Pct Recovery = 109% Analysis Date = 09/29/15 Pct Recovery = 109% Analysis Date = 09/24/15 Pct Recovery = 109% Analysis Date = 09/24/15 Pct Recovery = 109% Analysis Date = 09/19/15 Pct Recovery = 109% Analysis Date = 09/19/15 Pct Recovery = 109% Analysis Date = 09/14/15 Pct Recovery = 108% Analysis Date = 09/14/15 Pct Recovery = 108% Analysis Date = 09/10/15 Pct Recovery = 108% Analysis Date = 09/10/15 Pct Recovery = 108% Analysis Date = 09/05/15 Pct Recovery = 108% Analysis Date = 09/05/15 Pct Recovery = 108% Analysis Date = 08/31/15 Pct Recovery = 108% Analysis Date = 08/31/15 Pct Recovery = 108% Analysis Date = 08/26/15 Pct Recovery = 108% Analysis Date = 08/26/15 Pct Recovery = 108% Analysis Date = 08/21/15 Pct Recovery = 108% Analysis Date = 08/21/15 Pct Recovery = 108% Analysis Date = 08/17/15 Pct Recovery = 107% Analysis Date = 08/17/15 Pct Recovery = 107% Analysis Date = 08/12/15 Pct Recovery = 107% Analysis Date = 08/12/15 Pct Recovery = 107% Analysis Date = 08/07/15 Pct Recovery = 107% Analysis Date = 08/07/15 Pct Recovery = 107% Analysis Date = 08/02/15 Pct Recovery = 107% Analysis Date = 08/02/15 Pct Recovery = 107% Analysis Date = 07/29/15 Pct Recovery = 107% Analysis Date = 07/29/15 Pct Recovery = 107% Analysis Date = 07/24/15 Pct Recovery = 107% Analysis Date = 07/24/15 Pct Recovery = 107% Analysis Date = 07/19/15 Pct Recovery = 106% Analysis Date = 07/19/15 Pct Recovery = 106% Analysis Date = 07/14/15 Pct Recovery = 106% Analysis Date = 07/14/15 Pct Recovery = 106% Analysis Date = 07/09/15 Pct Recovery = 106% Analysis Date = 07/09/15 Pct Recovery = 106% Analysis Date = 07/05/15 Pct Recovery = 106% Analysis Date = 07/05/15 Pct Recovery = 106% Analysis Date = 06/30/15 Pct Recovery = 106% Analysis Date = 06/30/15 Pct Recovery = 106% Analysis Date = 06/25/15 Pct Recovery = 106% Analysis Date = 06/25/15 Pct Recovery = 106% Analysis Date = 06/20/15 Pct Recovery = 106% Analysis Date = 06/20/15 Pct Recovery = 106% Analysis Date = 06/16/15 Pct Recovery = 106% Analysis Date = 06/16/15 Pct Recovery = 106% Analysis Date = 06/11/15 Pct Recovery = 105% Analysis Date = 06/11/15 Pct Recovery = 105% Analysis Date = 06/06/15 Pct Recovery = 105% Analysis Date = 06/06/15 Pct Recovery = 105% Analysis Date = 06/01/15 Pct Recovery = 105% Analysis Date = 06/01/15 Pct Recovery = 105% Analysis Date = 05/27/15 Pct Recovery = 105% Analysis Date = 05/27/15 Pct Recovery = 105% Analysis Date = 05/23/15 Pct Recovery = 105% Analysis Date = 05/23/15 Pct Recovery = 105% Analysis Date = 05/18/15 Pct Recovery = 105% Analysis Date = 05/18/15 Pct Recovery = 105% Analysis Date = 05/13/15 Pct Recovery = 105% Analysis Date = 05/13/15 Pct Recovery = 105% Analysis Date = 05/08/15 Pct Recovery = 105% Analysis Date = 05/08/15 Pct Recovery = 105% Analysis Date = 05/04/15 Pct Recovery = 105% Analysis Date = 05/04/15 Pct Recovery = 105% Analysis Date = 04/29/15 Pct Recovery = 105% Analysis Date = 04/29/15 Pct Recovery = 105% Analysis Date = 04/24/15 Pct Recovery = 105% Analysis Date = 04/24/15 Pct Recovery = 105% Analysis Date = 04/19/15 Pct Recovery = 105% Analysis Date = 04/19/15 Pct Recovery = 105% Analysis Date = 04/14/15 Pct Recovery = 105% Analysis Date = 04/14/15 Pct Recovery = 105% Analysis Date = 04/10/15 Pct Recovery = 105% Analysis Date = 04/10/15 Pct Recovery = 105% Analysis Date = 04/05/15 Pct Recovery = 105% Analysis Date = 04/05/15 Pct Recovery = 105% Analysis Date = 03/31/15 Pct Recovery = 105% Analysis Date = 03/31/15 Pct Recovery = 105% Analysis Date = 03/26/15 Pct Recovery = 105% Analysis Date = 03/26/15 Pct Recovery = 105% Analysis Date = 03/22/15 Pct Recovery = 105% Analysis Date = 03/22/15 Pct Recovery = 105% Analysis Date = 03/17/15 Pct Recovery = 105% Analysis Date = 03/17/15 Pct Recovery = 105% Analysis Date = 03/12/15 Pct Recovery = 105% Analysis Date = 03/12/15 Pct Recovery = 105% Analysis Date = 03/07/15 Pct Recovery = 105% Analysis Date = 03/07/15 Pct Recovery = 105% Analysis Date = 03/02/15 Pct Recovery = 105% Analysis Date = 03/02/15 Pct Recovery = 105% Analysis Date = 02/26/15 Pct Recovery = 105% Analysis Date = 02/26/15 Pct Recovery = 105% Analysis Date = 02/21/15 Pct Recovery = 105% Analysis Date = 02/21/15 Pct Recovery = 105% Analysis Date = 02/16/15 Pct Recovery = 105% Analysis Date = 02/16/15 Pct Recovery = 105% Analysis Date = 02/11/15 Pct Recovery = 105% Analysis Date = 02/11/15 Pct Recovery = 105% Analysis Date = 02/07/15 Pct Recovery = 105% Analysis Date = 02/07/15 Pct Recovery = 105% Analysis Date = 02/02/15 Pct Recovery = 105% Analysis Date = 02/02/15 Pct Recovery = 105% Analysis Date = 01/28/15 Pct Recovery = 105% Analysis Date = 01/28/15 Pct Recovery = 105% Analysis Date = 01/23/15 Pct Recovery = 105% Analysis Date = 01/23/15 Pct Recovery = 105% Analysis Date = 01/18/15 Pct Recovery = 105% Analysis Date = 01/18/15 Pct Recovery = 105% Analysis Date = 01/14/15 Pct Recovery = 105% Analysis Date = 01/14/15 Pct Recovery = 105% Analysis Date = 01/09/15 Pct Recovery = 105% Analysis Date = 01/09/15 Pct Recovery = 105% Analysis Date = 01/04/15 Pct Recovery = 105% Analysis Date = 01/04/15 Pct Recovery = 105% Analysis Date = 12/30/14 Pct Recovery = 105% Analysis Date = 12/30/14 Pct Recovery = 105% Analysis Date = 12/25/14 Pct Recovery = 105% Analysis Date = 12/25/14 Pct Recovery = 105% Analysis Date = 12/21/14 Pct Recovery = 105% Analysis Date = 12/21/14 Pct Recovery = 105% Analysis Date = 12/16/14 Pct Recovery = 105% Analysis Date = 12/16/14 Pct Recovery = 105% Analysis Date = 12/11/14 Pct Recovery = 106% Analysis Date = 12/11/14 Pct Recovery = 106% Analysis Date = 12/06/14 Pct Recovery = 106% Analysis Date = 12/06/14 Pct Recovery = 106% Analysis Date = 12/02/14 Pct Recovery = 106% Analysis Date = 12/02/14 Pct Recovery = 106% Analysis Date = 11/27/14 Pct Recovery = 106% Analysis Date = 11/27/14 Pct Recovery = 106% Analysis Date = 11/22/14 Pct Recovery = 106% Analysis Date = 11/22/14 Pct Recovery = 106% Analysis Date = 11/17/14 Pct Recovery = 106% Analysis Date = 11/17/14 Pct Recovery = 106% Analysis Date = 11/12/14 Pct Recovery = 106% Analysis Date = 11/12/14 Pct Recovery = 106% Analysis Date = 11/08/14 Pct Recovery = 107% Analysis Date = 11/08/14 Pct Recovery = 107% Analysis Date = 11/03/14 Pct Recovery = 107% Analysis Date = 11/03/14 Pct Recovery = 107% Analysis Date = 10/29/14 Pct Recovery = 107% Analysis Date = 10/29/14 Pct Recovery = 107% Analysis Date = 10/24/14 Pct Recovery = 107% Analysis Date = 10/24/14 Pct Recovery = 107% Analysis Date = 10/20/14 Pct Recovery = 107% Analysis Date = 10/20/14 Pct Recovery = 107% Analysis Date = 10/15/14 Pct Recovery = 107% Analysis Date = 10/15/14 Pct Recovery = 107% Analysis Date = 10/10/14 Pct Recovery = 107% Analysis Date = 10/10/14 Pct Recovery = 107% Analysis Date = 10/05/14 Pct Recovery = 108% Analysis Date = 10/05/14 Pct Recovery = 108% Analysis Date = 09/30/14 Pct Recovery = 108% Analysis Date = 09/30/14 Pct Recovery = 108% Analysis Date = 09/26/14 Pct Recovery = 108% Analysis Date = 09/26/14 Pct Recovery = 108% Analysis Date = 09/21/14 Pct Recovery = 108% Analysis Date = 09/21/14 Pct Recovery = 108% Analysis Date = 09/16/14 Pct Recovery = 108% Analysis Date = 09/16/14 Pct Recovery = 108% Analysis Date = 09/11/14 Pct Recovery = 108% Analysis Date = 09/11/14 Pct Recovery = 108% Analysis Date = 09/07/14 Pct Recovery = 109% Analysis Date = 09/07/14 Pct Recovery = 109% Analysis Date = 09/02/14 Pct Recovery = 109% Analysis Date = 09/02/14 Pct Recovery = 109% Analysis Date = 08/28/14 Pct Recovery = 109% Analysis Date = 08/28/14 Pct Recovery = 109% Analysis Date = 08/23/14 Pct Recovery = 109% Analysis Date = 08/23/14 Pct Recovery = 109% Analysis Date = 08/18/14 Pct Recovery = 109% Analysis Date = 08/18/14 Pct Recovery = 109% Analysis Date = 08/14/14 Pct Recovery = 109% Analysis Date = 08/14/14 Pct Recovery = 109% Analysis Date = 08/09/14 Pct Recovery = 110% Analysis Date = 08/09/14 Pct Recovery = 110% Analysis Date = 08/04/14 Pct Recovery = 110% Analysis Date = 08/04/14 Pct Recovery = 110% Analysis Date = 07/30/14 Pct Recovery = 110% Analysis Date = 07/30/14 Pct Recovery = 110% Analysis Date = 07/26/14 Pct Recovery = 110% Analysis Date = 07/26/14 Pct Recovery = 110% Analysis Date = 07/21/14 Pct Recovery = 110% Analysis Date = 07/21/14 Pct Recovery = 110% Analysis Date = 07/16/14 Pct Recovery = 111% Analysis Date = 07/16/14 Pct Recovery = 111% Analysis Date = 07/11/14 Pct Recovery = 111% Analysis Date = 07/11/14 Pct Recovery = 111% Analysis Date = 07/06/14 Pct Recovery = 111% Analysis Date = 07/06/14 Pct Recovery = 111% Analysis Date = 07/02/14 Pct Recovery = 111% Analysis Date = 07/02/14 Pct Recovery = 111% Analysis Date = 06/27/14 Pct Recovery = 111% Analysis Date = 06/27/14 Pct Recovery = 111% Analysis Date = 06/22/14 Pct Recovery = 112% Analysis Date = 06/22/14 Pct Recovery = 112% Analysis Date = 06/17/14 Pct Recovery = 112% Analysis Date = 06/17/14 Pct Recovery = 112% Analysis Date = 06/13/14 Pct Recovery = 112% Analysis Date = 06/13/14 Pct Recovery = 112% Analysis Date = 06/08/14 Pct Recovery = 112% Analysis Date = 06/08/14 Pct Recovery = 112% Analysis Date = 06/03/14 Pct Recovery = 112% Analysis Date = 06/03/14 Pct Recovery = 112% Analysis Date = 05/29/14 Pct Recovery = 113% Analysis Date = 05/29/14 Pct Recovery = 113% Analysis Date = 05/24/14 Pct Recovery = 113% Analysis Date = 05/24/14 Pct Recovery = 113% Analysis Date = 05/20/14 Pct Recovery = 113% Analysis Date = 05/20/14 Pct Recovery = 113% Analysis Date = 05/15/14 Pct Recovery = 113% Analysis Date = 05/15/14 Pct Recovery = 113% Analysis Date = 05/10/14 Pct Recovery = 113% Analysis Date = 05/10/14 Pct Recovery = 113% Analysis Date = 05/05/14 Pct Recovery = 114% Analysis Date = 05/05/14 Pct Recovery = 114% Analysis Date = 05/01/14 Pct Recovery = 114% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
TRICHLOROETHYLENE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 48 107% 18% 104% 16%
Total 48 107% 18% 104% 16%

Sample Statistics
TRICHLOROETHYLENE

Characteristic N % % Basis
Plotted 48 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 48 .  
False Negatives 0 0% 0 out of 48
Not Spiked 25 .  
False Positives 5 20% 5 out of 25

BQS OBSP Determination:
TRICHLOROFLUOROMETHANE
METHOD: 4440 , TESTIDCODE: 34488GCM66
Open Data Set

Analysis Date = 12/16/16 SpikeMix = NSI 041816AVOC: 40 µl & ChemService 5082900: 40 µl Pct Recovery = 87% Analysis Date = 12/12/16 SpikeMix = Accu 216041125: 40 µl & Crescent 03FF058: 40 µl Pct Recovery = 85% Analysis Date = 08/04/16 SpikeMix = Crescent 03FF058: 40 µl & Supelco LC20141V: 40 µl Pct Recovery = 96% Analysis Date = 07/14/16 SpikeMix = Accu 216041125: 40 µl & NSI 041816AVOC: 40 µl Pct Recovery = 95% Analysis Date = 11/21/16 SpikeMix = Crescent 03FF058: 25 µl & Supelco LC20141V: 25 µl Pct Recovery = 75% Analysis Date = 08/26/16 SpikeMix = NSI 041816AVOC: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 95% Analysis Date = 06/30/16 SpikeMix = Crescent 03FF058: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 92% Analysis Date = 06/21/16 SpikeMix = Phenova B20160319: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 82% Analysis Date = 05/24/16 SpikeMix = Accu 216041125: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 80% Analysis Date = 03/19/15 SpikeMix = Spex Organics C1140417015: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 111% Analysis Date = 03/06/15 SpikeMix = ERA 0227-14-06.1A: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 99% Analysis Date = 12/17/14 SpikeMix = Supelco LC06438: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 100% Analysis Date = 11/22/14 SpikeMix = NSI 032614: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 124% Analysis Date = 09/21/14 SpikeMix = Supelco LC06438: 20 µl Pct Recovery = 107% Analysis Date = 08/19/14 SpikeMix = Spex Organics C1140417015: 20 µl & Accu 214031115: 20 µl Pct Recovery = 128% Analysis Date = 08/16/14 SpikeMix = ERA 0227-14-06.1A: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 129% Analysis Date = 06/10/14 SpikeMix = NSI 032614: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 109% Analysis Date = 08/15/15 SpikeMix = Supelco LC13545: 25 µl & Crescent 04EE008: 25 µl Pct Recovery = 95% Analysis Date = 06/16/15 SpikeMix = ERA 0406-15-03: 25 µl & Supelco LC13545: 25 µl Pct Recovery = 87% Analysis Date = 10/13/16 SpikeMix = Accu 216041125: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 89% Analysis Date = 10/13/16 SpikeMix = NSI 041816AVOC: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 86% Analysis Date = 09/28/16 SpikeMix = Crescent 03FF058: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 85% Analysis Date = 09/08/16 SpikeMix = Phenova B20160319: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 89% Analysis Date = 08/20/16 SpikeMix = Accu 216041125: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 89% Analysis Date = 07/29/16 SpikeMix = Phenova B20160319: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 88% Analysis Date = 06/10/16 SpikeMix = NSI 041816AVOC: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 91% Analysis Date = 04/26/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 81% Analysis Date = 02/05/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 95% Analysis Date = 11/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 81% Analysis Date = 10/16/15 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 90% Analysis Date = 05/09/15 SpikeMix = Spex Organics EN150428007: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 101% Analysis Date = 04/02/16 SpikeMix = Supelco LC13545: 15 µl & Accu 215041380: 15 µl Pct Recovery = 112% Analysis Date = 12/18/15 SpikeMix = Supelco LC13545: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 89% Analysis Date = 11/06/14 SpikeMix = Spex Organics C1140417015: 10 µl & Crescent 03DD004: 10 µl Pct Recovery = 107% Analysis Date = 10/21/14 SpikeMix = ERA 0227-14-06.1A: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 100% Analysis Date = 09/09/14 SpikeMix = NSI 032614: 10 µl & Spex Organics C1140417015: 10 µl Pct Recovery = 126% Analysis Date = 07/23/14 SpikeMix = Spex Organics C1140417015: 10 µl & Accu 214031115: 10 µl Pct Recovery = 137% Analysis Date = 07/11/14 SpikeMix = Spex Organics C1140417015: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 117% Analysis Date = 06/18/14 SpikeMix = Supelco LC06438: 10 µl & Accu 214031115: 10 µl Pct Recovery = 112% Analysis Date = 05/30/14 SpikeMix = NSI 032614: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 99% Analysis Date = 05/03/14 SpikeMix = Crescent 03DD004: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 108% Analysis Date = 02/18/16 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 102% Analysis Date = 11/12/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 102% Analysis Date = 09/03/15 SpikeMix = NSI 050515AVOC: 10 µl & Spex Organics EN150428007: 10 µl Pct Recovery = 86% Analysis Date = 05/21/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 102% Analysis Date = 05/13/16 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 93% Analysis Date = 03/17/16 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 98% Analysis Date = 12/10/15 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 89% Analysis Date = 06/27/15 SpikeMix = ERA 0406-15-03: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 96% Analysis Date = 05/09/15 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 97% Analysis Date = 12/16/16 Pct Recovery = 85% Analysis Date = 12/11/16 Pct Recovery = 85% Analysis Date = 12/11/16 Pct Recovery = 85% Analysis Date = 12/06/16 Pct Recovery = 85% Analysis Date = 12/06/16 Pct Recovery = 85% Analysis Date = 12/01/16 Pct Recovery = 85% Analysis Date = 12/01/16 Pct Recovery = 85% Analysis Date = 11/26/16 Pct Recovery = 86% Analysis Date = 11/26/16 Pct Recovery = 86% Analysis Date = 11/22/16 Pct Recovery = 86% Analysis Date = 11/22/16 Pct Recovery = 86% Analysis Date = 11/17/16 Pct Recovery = 86% Analysis Date = 11/17/16 Pct Recovery = 86% Analysis Date = 11/12/16 Pct Recovery = 86% Analysis Date = 11/12/16 Pct Recovery = 86% Analysis Date = 11/07/16 Pct Recovery = 86% Analysis Date = 11/07/16 Pct Recovery = 86% Analysis Date = 11/02/16 Pct Recovery = 86% Analysis Date = 11/02/16 Pct Recovery = 86% Analysis Date = 10/29/16 Pct Recovery = 86% Analysis Date = 10/29/16 Pct Recovery = 86% Analysis Date = 10/24/16 Pct Recovery = 87% Analysis Date = 10/24/16 Pct Recovery = 87% Analysis Date = 10/19/16 Pct Recovery = 87% Analysis Date = 10/19/16 Pct Recovery = 87% Analysis Date = 10/14/16 Pct Recovery = 87% Analysis Date = 10/14/16 Pct Recovery = 87% Analysis Date = 10/09/16 Pct Recovery = 87% Analysis Date = 10/09/16 Pct Recovery = 87% Analysis Date = 10/05/16 Pct Recovery = 87% Analysis Date = 10/05/16 Pct Recovery = 87% Analysis Date = 09/30/16 Pct Recovery = 87% Analysis Date = 09/30/16 Pct Recovery = 87% Analysis Date = 09/25/16 Pct Recovery = 88% Analysis Date = 09/25/16 Pct Recovery = 88% Analysis Date = 09/20/16 Pct Recovery = 88% Analysis Date = 09/20/16 Pct Recovery = 88% Analysis Date = 09/15/16 Pct Recovery = 88% Analysis Date = 09/15/16 Pct Recovery = 88% Analysis Date = 09/11/16 Pct Recovery = 88% Analysis Date = 09/11/16 Pct Recovery = 88% Analysis Date = 09/06/16 Pct Recovery = 88% Analysis Date = 09/06/16 Pct Recovery = 88% Analysis Date = 09/01/16 Pct Recovery = 88% Analysis Date = 09/01/16 Pct Recovery = 88% Analysis Date = 08/27/16 Pct Recovery = 88% Analysis Date = 08/27/16 Pct Recovery = 88% Analysis Date = 08/23/16 Pct Recovery = 89% Analysis Date = 08/23/16 Pct Recovery = 89% Analysis Date = 08/18/16 Pct Recovery = 89% Analysis Date = 08/18/16 Pct Recovery = 89% Analysis Date = 08/13/16 Pct Recovery = 89% Analysis Date = 08/13/16 Pct Recovery = 89% Analysis Date = 08/08/16 Pct Recovery = 89% Analysis Date = 08/08/16 Pct Recovery = 89% Analysis Date = 08/03/16 Pct Recovery = 89% Analysis Date = 08/03/16 Pct Recovery = 89% Analysis Date = 07/30/16 Pct Recovery = 89% Analysis Date = 07/30/16 Pct Recovery = 89% Analysis Date = 07/25/16 Pct Recovery = 89% Analysis Date = 07/25/16 Pct Recovery = 89% Analysis Date = 07/20/16 Pct Recovery = 89% Analysis Date = 07/20/16 Pct Recovery = 89% Analysis Date = 07/15/16 Pct Recovery = 90% Analysis Date = 07/15/16 Pct Recovery = 90% Analysis Date = 07/10/16 Pct Recovery = 90% Analysis Date = 07/10/16 Pct Recovery = 90% Analysis Date = 07/06/16 Pct Recovery = 90% Analysis Date = 07/06/16 Pct Recovery = 90% Analysis Date = 07/01/16 Pct Recovery = 90% Analysis Date = 07/01/16 Pct Recovery = 90% Analysis Date = 06/26/16 Pct Recovery = 90% Analysis Date = 06/26/16 Pct Recovery = 90% Analysis Date = 06/21/16 Pct Recovery = 90% Analysis Date = 06/21/16 Pct Recovery = 90% Analysis Date = 06/16/16 Pct Recovery = 90% Analysis Date = 06/16/16 Pct Recovery = 90% Analysis Date = 06/12/16 Pct Recovery = 90% Analysis Date = 06/12/16 Pct Recovery = 90% Analysis Date = 06/07/16 Pct Recovery = 91% Analysis Date = 06/07/16 Pct Recovery = 91% Analysis Date = 06/02/16 Pct Recovery = 91% Analysis Date = 06/02/16 Pct Recovery = 91% Analysis Date = 05/28/16 Pct Recovery = 91% Analysis Date = 05/28/16 Pct Recovery = 91% Analysis Date = 05/24/16 Pct Recovery = 91% Analysis Date = 05/24/16 Pct Recovery = 91% Analysis Date = 05/19/16 Pct Recovery = 91% Analysis Date = 05/19/16 Pct Recovery = 91% Analysis Date = 05/14/16 Pct Recovery = 91% Analysis Date = 05/14/16 Pct Recovery = 91% Analysis Date = 05/09/16 Pct Recovery = 91% Analysis Date = 05/09/16 Pct Recovery = 91% Analysis Date = 05/04/16 Pct Recovery = 91% Analysis Date = 05/04/16 Pct Recovery = 91% Analysis Date = 04/30/16 Pct Recovery = 91% Analysis Date = 04/30/16 Pct Recovery = 91% Analysis Date = 04/25/16 Pct Recovery = 91% Analysis Date = 04/25/16 Pct Recovery = 91% Analysis Date = 04/20/16 Pct Recovery = 92% Analysis Date = 04/20/16 Pct Recovery = 92% Analysis Date = 04/15/16 Pct Recovery = 92% Analysis Date = 04/15/16 Pct Recovery = 92% Analysis Date = 04/10/16 Pct Recovery = 92% Analysis Date = 04/10/16 Pct Recovery = 92% Analysis Date = 04/06/16 Pct Recovery = 92% Analysis Date = 04/06/16 Pct Recovery = 92% Analysis Date = 04/01/16 Pct Recovery = 92% Analysis Date = 04/01/16 Pct Recovery = 92% Analysis Date = 03/27/16 Pct Recovery = 92% Analysis Date = 03/27/16 Pct Recovery = 92% Analysis Date = 03/22/16 Pct Recovery = 92% Analysis Date = 03/22/16 Pct Recovery = 92% Analysis Date = 03/17/16 Pct Recovery = 92% Analysis Date = 03/17/16 Pct Recovery = 92% Analysis Date = 03/13/16 Pct Recovery = 92% Analysis Date = 03/13/16 Pct Recovery = 92% Analysis Date = 03/08/16 Pct Recovery = 92% Analysis Date = 03/08/16 Pct Recovery = 92% Analysis Date = 03/03/16 Pct Recovery = 92% Analysis Date = 03/03/16 Pct Recovery = 92% Analysis Date = 02/27/16 Pct Recovery = 92% Analysis Date = 02/27/16 Pct Recovery = 92% Analysis Date = 02/23/16 Pct Recovery = 92% Analysis Date = 02/23/16 Pct Recovery = 92% Analysis Date = 02/18/16 Pct Recovery = 92% Analysis Date = 02/18/16 Pct Recovery = 92% Analysis Date = 02/13/16 Pct Recovery = 92% Analysis Date = 02/13/16 Pct Recovery = 92% Analysis Date = 02/08/16 Pct Recovery = 92% Analysis Date = 02/08/16 Pct Recovery = 92% Analysis Date = 02/03/16 Pct Recovery = 92% Analysis Date = 02/03/16 Pct Recovery = 92% Analysis Date = 01/30/16 Pct Recovery = 92% Analysis Date = 01/30/16 Pct Recovery = 92% Analysis Date = 01/25/16 Pct Recovery = 92% Analysis Date = 01/25/16 Pct Recovery = 92% Analysis Date = 01/20/16 Pct Recovery = 92% Analysis Date = 01/20/16 Pct Recovery = 92% Analysis Date = 01/15/16 Pct Recovery = 92% Analysis Date = 01/15/16 Pct Recovery = 92% Analysis Date = 01/10/16 Pct Recovery = 93% Analysis Date = 01/10/16 Pct Recovery = 93% Analysis Date = 01/06/16 Pct Recovery = 93% Analysis Date = 01/06/16 Pct Recovery = 93% Analysis Date = 01/01/16 Pct Recovery = 93% Analysis Date = 01/01/16 Pct Recovery = 93% Analysis Date = 12/27/15 Pct Recovery = 93% Analysis Date = 12/27/15 Pct Recovery = 93% Analysis Date = 12/22/15 Pct Recovery = 93% Analysis Date = 12/22/15 Pct Recovery = 93% Analysis Date = 12/17/15 Pct Recovery = 93% Analysis Date = 12/17/15 Pct Recovery = 93% Analysis Date = 12/13/15 Pct Recovery = 93% Analysis Date = 12/13/15 Pct Recovery = 93% Analysis Date = 12/08/15 Pct Recovery = 93% Analysis Date = 12/08/15 Pct Recovery = 93% Analysis Date = 12/03/15 Pct Recovery = 93% Analysis Date = 12/03/15 Pct Recovery = 93% Analysis Date = 11/28/15 Pct Recovery = 93% Analysis Date = 11/28/15 Pct Recovery = 93% Analysis Date = 11/24/15 Pct Recovery = 93% Analysis Date = 11/24/15 Pct Recovery = 93% Analysis Date = 11/19/15 Pct Recovery = 93% Analysis Date = 11/19/15 Pct Recovery = 93% Analysis Date = 11/14/15 Pct Recovery = 93% Analysis Date = 11/14/15 Pct Recovery = 93% Analysis Date = 11/09/15 Pct Recovery = 93% Analysis Date = 11/09/15 Pct Recovery = 93% Analysis Date = 11/04/15 Pct Recovery = 93% Analysis Date = 11/04/15 Pct Recovery = 93% Analysis Date = 10/31/15 Pct Recovery = 94% Analysis Date = 10/31/15 Pct Recovery = 94% Analysis Date = 10/26/15 Pct Recovery = 94% Analysis Date = 10/26/15 Pct Recovery = 94% Analysis Date = 10/21/15 Pct Recovery = 94% Analysis Date = 10/21/15 Pct Recovery = 94% Analysis Date = 10/16/15 Pct Recovery = 94% Analysis Date = 10/16/15 Pct Recovery = 94% Analysis Date = 10/11/15 Pct Recovery = 94% Analysis Date = 10/11/15 Pct Recovery = 94% Analysis Date = 10/07/15 Pct Recovery = 94% Analysis Date = 10/07/15 Pct Recovery = 94% Analysis Date = 10/02/15 Pct Recovery = 95% Analysis Date = 10/02/15 Pct Recovery = 95% Analysis Date = 09/27/15 Pct Recovery = 95% Analysis Date = 09/27/15 Pct Recovery = 95% Analysis Date = 09/22/15 Pct Recovery = 95% Analysis Date = 09/22/15 Pct Recovery = 95% Analysis Date = 09/17/15 Pct Recovery = 95% Analysis Date = 09/17/15 Pct Recovery = 95% Analysis Date = 09/13/15 Pct Recovery = 95% Analysis Date = 09/13/15 Pct Recovery = 95% Analysis Date = 09/08/15 Pct Recovery = 95% Analysis Date = 09/08/15 Pct Recovery = 95% Analysis Date = 09/03/15 Pct Recovery = 95% Analysis Date = 09/03/15 Pct Recovery = 95% Analysis Date = 08/29/15 Pct Recovery = 96% Analysis Date = 08/29/15 Pct Recovery = 96% Analysis Date = 08/25/15 Pct Recovery = 96% Analysis Date = 08/25/15 Pct Recovery = 96% Analysis Date = 08/20/15 Pct Recovery = 96% Analysis Date = 08/20/15 Pct Recovery = 96% Analysis Date = 08/15/15 Pct Recovery = 96% Analysis Date = 08/15/15 Pct Recovery = 96% Analysis Date = 08/10/15 Pct Recovery = 96% Analysis Date = 08/10/15 Pct Recovery = 96% Analysis Date = 08/05/15 Pct Recovery = 96% Analysis Date = 08/05/15 Pct Recovery = 96% Analysis Date = 08/01/15 Pct Recovery = 96% Analysis Date = 08/01/15 Pct Recovery = 96% Analysis Date = 07/27/15 Pct Recovery = 97% Analysis Date = 07/27/15 Pct Recovery = 97% Analysis Date = 07/22/15 Pct Recovery = 97% Analysis Date = 07/22/15 Pct Recovery = 97% Analysis Date = 07/17/15 Pct Recovery = 97% Analysis Date = 07/17/15 Pct Recovery = 97% Analysis Date = 07/12/15 Pct Recovery = 97% Analysis Date = 07/12/15 Pct Recovery = 97% Analysis Date = 07/08/15 Pct Recovery = 97% Analysis Date = 07/08/15 Pct Recovery = 97% Analysis Date = 07/03/15 Pct Recovery = 97% Analysis Date = 07/03/15 Pct Recovery = 97% Analysis Date = 06/28/15 Pct Recovery = 98% Analysis Date = 06/28/15 Pct Recovery = 98% Analysis Date = 06/23/15 Pct Recovery = 98% Analysis Date = 06/23/15 Pct Recovery = 98% Analysis Date = 06/18/15 Pct Recovery = 98% Analysis Date = 06/18/15 Pct Recovery = 98% Analysis Date = 06/14/15 Pct Recovery = 98% Analysis Date = 06/14/15 Pct Recovery = 98% Analysis Date = 06/09/15 Pct Recovery = 98% Analysis Date = 06/09/15 Pct Recovery = 98% Analysis Date = 06/04/15 Pct Recovery = 98% Analysis Date = 06/04/15 Pct Recovery = 98% Analysis Date = 05/30/15 Pct Recovery = 98% Analysis Date = 05/30/15 Pct Recovery = 98% Analysis Date = 05/25/15 Pct Recovery = 99% Analysis Date = 05/25/15 Pct Recovery = 99% Analysis Date = 05/21/15 Pct Recovery = 99% Analysis Date = 05/21/15 Pct Recovery = 99% Analysis Date = 05/16/15 Pct Recovery = 99% Analysis Date = 05/16/15 Pct Recovery = 99% Analysis Date = 05/11/15 Pct Recovery = 99% Analysis Date = 05/11/15 Pct Recovery = 99% Analysis Date = 05/06/15 Pct Recovery = 100% Analysis Date = 05/06/15 Pct Recovery = 100% Analysis Date = 05/02/15 Pct Recovery = 100% Analysis Date = 05/02/15 Pct Recovery = 100% Analysis Date = 04/27/15 Pct Recovery = 100% Analysis Date = 04/27/15 Pct Recovery = 100% Analysis Date = 04/22/15 Pct Recovery = 100% Analysis Date = 04/22/15 Pct Recovery = 100% Analysis Date = 04/17/15 Pct Recovery = 101% Analysis Date = 04/17/15 Pct Recovery = 101% Analysis Date = 04/12/15 Pct Recovery = 101% Analysis Date = 04/12/15 Pct Recovery = 101% Analysis Date = 04/08/15 Pct Recovery = 101% Analysis Date = 04/08/15 Pct Recovery = 101% Analysis Date = 04/03/15 Pct Recovery = 102% Analysis Date = 04/03/15 Pct Recovery = 102% Analysis Date = 03/29/15 Pct Recovery = 102% Analysis Date = 03/29/15 Pct Recovery = 102% Analysis Date = 03/24/15 Pct Recovery = 102% Analysis Date = 03/24/15 Pct Recovery = 102% Analysis Date = 03/19/15 Pct Recovery = 102% Analysis Date = 03/19/15 Pct Recovery = 102% Analysis Date = 03/15/15 Pct Recovery = 103% Analysis Date = 03/15/15 Pct Recovery = 103% Analysis Date = 03/10/15 Pct Recovery = 103% Analysis Date = 03/10/15 Pct Recovery = 103% Analysis Date = 03/05/15 Pct Recovery = 103% Analysis Date = 03/05/15 Pct Recovery = 103% Analysis Date = 02/28/15 Pct Recovery = 103% Analysis Date = 02/28/15 Pct Recovery = 103% Analysis Date = 02/23/15 Pct Recovery = 104% Analysis Date = 02/23/15 Pct Recovery = 104% Analysis Date = 02/19/15 Pct Recovery = 104% Analysis Date = 02/19/15 Pct Recovery = 104% Analysis Date = 02/14/15 Pct Recovery = 104% Analysis Date = 02/14/15 Pct Recovery = 104% Analysis Date = 02/09/15 Pct Recovery = 105% Analysis Date = 02/09/15 Pct Recovery = 105% Analysis Date = 02/04/15 Pct Recovery = 105% Analysis Date = 02/04/15 Pct Recovery = 105% Analysis Date = 01/31/15 Pct Recovery = 105% Analysis Date = 01/31/15 Pct Recovery = 105% Analysis Date = 01/26/15 Pct Recovery = 105% Analysis Date = 01/26/15 Pct Recovery = 105% Analysis Date = 01/21/15 Pct Recovery = 106% Analysis Date = 01/21/15 Pct Recovery = 106% Analysis Date = 01/16/15 Pct Recovery = 106% Analysis Date = 01/16/15 Pct Recovery = 106% Analysis Date = 01/11/15 Pct Recovery = 106% Analysis Date = 01/11/15 Pct Recovery = 106% Analysis Date = 01/07/15 Pct Recovery = 106% Analysis Date = 01/07/15 Pct Recovery = 106% Analysis Date = 01/02/15 Pct Recovery = 107% Analysis Date = 01/02/15 Pct Recovery = 107% Analysis Date = 12/28/14 Pct Recovery = 107% Analysis Date = 12/28/14 Pct Recovery = 107% Analysis Date = 12/23/14 Pct Recovery = 107% Analysis Date = 12/23/14 Pct Recovery = 107% Analysis Date = 12/18/14 Pct Recovery = 108% Analysis Date = 12/18/14 Pct Recovery = 108% Analysis Date = 12/14/14 Pct Recovery = 108% Analysis Date = 12/14/14 Pct Recovery = 108% Analysis Date = 12/09/14 Pct Recovery = 108% Analysis Date = 12/09/14 Pct Recovery = 108% Analysis Date = 12/04/14 Pct Recovery = 108% Analysis Date = 12/04/14 Pct Recovery = 108% Analysis Date = 11/29/14 Pct Recovery = 109% Analysis Date = 11/29/14 Pct Recovery = 109% Analysis Date = 11/24/14 Pct Recovery = 109% Analysis Date = 11/24/14 Pct Recovery = 109% Analysis Date = 11/20/14 Pct Recovery = 109% Analysis Date = 11/20/14 Pct Recovery = 109% Analysis Date = 11/15/14 Pct Recovery = 109% Analysis Date = 11/15/14 Pct Recovery = 109% Analysis Date = 11/10/14 Pct Recovery = 110% Analysis Date = 11/10/14 Pct Recovery = 110% Analysis Date = 11/05/14 Pct Recovery = 110% Analysis Date = 11/05/14 Pct Recovery = 110% Analysis Date = 11/01/14 Pct Recovery = 110% Analysis Date = 11/01/14 Pct Recovery = 110% Analysis Date = 10/27/14 Pct Recovery = 110% Analysis Date = 10/27/14 Pct Recovery = 110% Analysis Date = 10/22/14 Pct Recovery = 111% Analysis Date = 10/22/14 Pct Recovery = 111% Analysis Date = 10/17/14 Pct Recovery = 111% Analysis Date = 10/17/14 Pct Recovery = 111% Analysis Date = 10/12/14 Pct Recovery = 111% Analysis Date = 10/12/14 Pct Recovery = 111% Analysis Date = 10/08/14 Pct Recovery = 111% Analysis Date = 10/08/14 Pct Recovery = 111% Analysis Date = 10/03/14 Pct Recovery = 112% Analysis Date = 10/03/14 Pct Recovery = 112% Analysis Date = 09/28/14 Pct Recovery = 112% Analysis Date = 09/28/14 Pct Recovery = 112% Analysis Date = 09/23/14 Pct Recovery = 112% Analysis Date = 09/23/14 Pct Recovery = 112% Analysis Date = 09/18/14 Pct Recovery = 112% Analysis Date = 09/18/14 Pct Recovery = 112% Analysis Date = 09/14/14 Pct Recovery = 113% Analysis Date = 09/14/14 Pct Recovery = 113% Analysis Date = 09/09/14 Pct Recovery = 113% Analysis Date = 09/09/14 Pct Recovery = 113% Analysis Date = 09/04/14 Pct Recovery = 113% Analysis Date = 09/04/14 Pct Recovery = 113% Analysis Date = 08/30/14 Pct Recovery = 113% Analysis Date = 08/30/14 Pct Recovery = 113% Analysis Date = 08/25/14 Pct Recovery = 114% Analysis Date = 08/25/14 Pct Recovery = 114% Analysis Date = 08/21/14 Pct Recovery = 114% Analysis Date = 08/21/14 Pct Recovery = 114% Analysis Date = 08/16/14 Pct Recovery = 114% Analysis Date = 08/16/14 Pct Recovery = 114% Analysis Date = 08/11/14 Pct Recovery = 114% Analysis Date = 08/11/14 Pct Recovery = 114% Analysis Date = 08/06/14 Pct Recovery = 114% Analysis Date = 08/06/14 Pct Recovery = 114% Analysis Date = 08/02/14 Pct Recovery = 115% Analysis Date = 08/02/14 Pct Recovery = 115% Analysis Date = 07/28/14 Pct Recovery = 115% Analysis Date = 07/28/14 Pct Recovery = 115% Analysis Date = 07/23/14 Pct Recovery = 115% Analysis Date = 07/23/14 Pct Recovery = 115% Analysis Date = 07/18/14 Pct Recovery = 115% Analysis Date = 07/18/14 Pct Recovery = 115% Analysis Date = 07/13/14 Pct Recovery = 116% Analysis Date = 07/13/14 Pct Recovery = 116% Analysis Date = 07/09/14 Pct Recovery = 116% Analysis Date = 07/09/14 Pct Recovery = 116% Analysis Date = 07/04/14 Pct Recovery = 116% Analysis Date = 07/04/14 Pct Recovery = 116% Analysis Date = 06/29/14 Pct Recovery = 116% Analysis Date = 06/29/14 Pct Recovery = 116% Analysis Date = 06/24/14 Pct Recovery = 117% Analysis Date = 06/24/14 Pct Recovery = 117% Analysis Date = 06/19/14 Pct Recovery = 117% Analysis Date = 06/19/14 Pct Recovery = 117% Analysis Date = 06/15/14 Pct Recovery = 117% Analysis Date = 06/15/14 Pct Recovery = 117% Analysis Date = 06/10/14 Pct Recovery = 117% Analysis Date = 06/10/14 Pct Recovery = 117% Analysis Date = 06/05/14 Pct Recovery = 118% Analysis Date = 06/05/14 Pct Recovery = 118% Analysis Date = 05/31/14 Pct Recovery = 118% Analysis Date = 05/31/14 Pct Recovery = 118% Analysis Date = 05/26/14 Pct Recovery = 118% Analysis Date = 05/26/14 Pct Recovery = 118% Analysis Date = 05/22/14 Pct Recovery = 118% Analysis Date = 05/22/14 Pct Recovery = 118% Analysis Date = 05/17/14 Pct Recovery = 118% Analysis Date = 05/17/14 Pct Recovery = 118% Analysis Date = 05/12/14 Pct Recovery = 119% Analysis Date = 05/12/14 Pct Recovery = 119% Analysis Date = 05/07/14 Pct Recovery = 119% Analysis Date = 05/07/14 Pct Recovery = 119% Analysis Date = 05/03/14 Pct Recovery = 119% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
TRICHLOROFLUOROMETHANE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 50 98% 14% 95% 13%
Total 50 98% 14% 95% 13%

Sample Statistics
TRICHLOROFLUOROMETHANE

Characteristic N % % Basis
Plotted 50 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 50 .  
False Negatives 0 0% 0 out of 50
Not Spiked 23 .  
False Positives 0 0% 0 out of 23

BQS OBSP Determination:
VINYL CHLORIDE
METHOD: 4440 , TESTIDCODE: 39175GCM66
Open Data Set

Analysis Date = 08/04/16 SpikeMix = Crescent 03FF058: 40 µl & Supelco LC20141V: 40 µl Pct Recovery = 83% Analysis Date = 07/20/16 SpikeMix = Supelco LC20141V: 40 µl & Accu 216041125: 40 µl Pct Recovery = 87% Analysis Date = 12/16/16 SpikeMix = NSI 041816AVOC: 40 µl & ChemService 5082900: 40 µl Pct Recovery = 109% Analysis Date = 11/21/16 SpikeMix = Crescent 03FF058: 25 µl & Supelco LC20141V: 25 µl Pct Recovery = 78% Analysis Date = 09/08/16 SpikeMix = Supelco LC20141V: 25 µl & Accu 216041125: 25 µl Pct Recovery = 72% Analysis Date = 04/09/15 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 78% Analysis Date = 08/19/14 SpikeMix = Spex Organics C1140417015: 20 µl & Accu 214031115: 20 µl Pct Recovery = 120% Analysis Date = 07/01/14 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 103% Analysis Date = 05/01/14 SpikeMix = Accu 214031115: 20 µl & NSI 032614: 20 µl Pct Recovery = 83% Analysis Date = 08/26/16 SpikeMix = NSI 041816AVOC: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 93% Analysis Date = 08/12/16 SpikeMix = ChemService 5082900: 25 µl & Phenova B20160319: 25 µl Pct Recovery = 98% Analysis Date = 06/30/16 SpikeMix = Crescent 03FF058: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 96% Analysis Date = 03/19/15 SpikeMix = Spex Organics C1140417015: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 90% Analysis Date = 12/17/14 SpikeMix = Supelco LC06438: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 94% Analysis Date = 11/14/14 SpikeMix = Crescent 03DD004: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 83% Analysis Date = 06/10/14 SpikeMix = Crescent 03DD004: 20 µl & NSI 032614: 20 µl Pct Recovery = 99% Analysis Date = 09/29/15 SpikeMix = Accu 215041380: 25 µl & ERA 0406-15-03: 25 µl Pct Recovery = 101% Analysis Date = 07/13/15 SpikeMix = Crescent 04EE008: 25 µl & NSI 050515AVOC: 25 µl Pct Recovery = 71% Analysis Date = 06/16/15 SpikeMix = ERA 0406-15-03: 25 µl & Supelco LC13545: 25 µl Pct Recovery = 93% Analysis Date = 10/13/16 SpikeMix = NSI 041816AVOC: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 81% Analysis Date = 05/27/16 SpikeMix = Phenova B20160319: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 81% Analysis Date = 11/29/16 SpikeMix = ChemService 5082900: 15 µl & Phenova B20160319: 15 µl Pct Recovery = 92% Analysis Date = 09/28/16 SpikeMix = Crescent 03FF058: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 101% Analysis Date = 06/30/16 SpikeMix = ChemService 5082900: 15 µl & Accu 216041125: 15 µl Pct Recovery = 103% Analysis Date = 06/10/16 SpikeMix = NSI 041816AVOC: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 100% Analysis Date = 04/26/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 82% Analysis Date = 03/04/16 SpikeMix = Accu 215041380: 15 µl & ERA 0406-15-03: 15 µl Pct Recovery = 101% Analysis Date = 02/05/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 110% Analysis Date = 11/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 70% Analysis Date = 10/17/15 SpikeMix = Crescent 04EE008: 15 µl & NSI 050515AVOC: 15 µl Pct Recovery = 65% Analysis Date = 10/16/15 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 89% Analysis Date = 06/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Accu 215041380: 15 µl Pct Recovery = 80% Analysis Date = 01/13/15 SpikeMix = Accu 214031115: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 108% Analysis Date = 09/09/14 SpikeMix = Accu 214031115: 10 µl & NSI 032614: 10 µl Pct Recovery = 118% Analysis Date = 07/23/14 SpikeMix = Spex Organics C1140417015: 10 µl & Accu 214031115: 10 µl Pct Recovery = 125% Analysis Date = 06/18/14 SpikeMix = Supelco LC06438: 10 µl & Accu 214031115: 10 µl Pct Recovery = 107% Analysis Date = 11/06/14 SpikeMix = Spex Organics C1140417015: 10 µl & Crescent 03DD004: 10 µl Pct Recovery = 76% Analysis Date = 10/04/14 SpikeMix = Crescent 03DD004: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 88% Analysis Date = 07/29/14 SpikeMix = Crescent 03DD004: 10 µl & NSI 032614: 10 µl Pct Recovery = 84% Analysis Date = 05/03/14 SpikeMix = Crescent 03DD004: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 99% Analysis Date = 03/17/16 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 72% Analysis Date = 01/27/16 SpikeMix = Crescent 04EE008: 10 µl & NSI 050515AVOC: 10 µl Pct Recovery = 84% Analysis Date = 12/10/15 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 84% Analysis Date = 11/20/15 SpikeMix = Accu 215041380: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 114% Analysis Date = 09/03/15 SpikeMix = NSI 050515AVOC: 10 µl & Spex Organics EN150428007: 10 µl Pct Recovery = 61% Analysis Date = 07/31/15 SpikeMix = Crescent 04EE008: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 96% Analysis Date = 06/27/15 SpikeMix = ERA 0406-15-03: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 112% Analysis Date = 12/15/16 Pct Recovery = 91% Analysis Date = 12/11/16 Pct Recovery = 91% Analysis Date = 12/11/16 Pct Recovery = 91% Analysis Date = 12/06/16 Pct Recovery = 91% Analysis Date = 12/06/16 Pct Recovery = 91% Analysis Date = 12/01/16 Pct Recovery = 91% Analysis Date = 12/01/16 Pct Recovery = 91% Analysis Date = 11/26/16 Pct Recovery = 91% Analysis Date = 11/26/16 Pct Recovery = 91% Analysis Date = 11/21/16 Pct Recovery = 91% Analysis Date = 11/21/16 Pct Recovery = 91% Analysis Date = 11/17/16 Pct Recovery = 91% Analysis Date = 11/17/16 Pct Recovery = 91% Analysis Date = 11/12/16 Pct Recovery = 91% Analysis Date = 11/12/16 Pct Recovery = 91% Analysis Date = 11/07/16 Pct Recovery = 91% Analysis Date = 11/07/16 Pct Recovery = 91% Analysis Date = 11/02/16 Pct Recovery = 91% Analysis Date = 11/02/16 Pct Recovery = 91% Analysis Date = 10/28/16 Pct Recovery = 91% Analysis Date = 10/28/16 Pct Recovery = 91% Analysis Date = 10/24/16 Pct Recovery = 91% Analysis Date = 10/24/16 Pct Recovery = 91% Analysis Date = 10/19/16 Pct Recovery = 91% Analysis Date = 10/19/16 Pct Recovery = 91% Analysis Date = 10/14/16 Pct Recovery = 91% Analysis Date = 10/14/16 Pct Recovery = 91% Analysis Date = 10/09/16 Pct Recovery = 91% Analysis Date = 10/09/16 Pct Recovery = 91% Analysis Date = 10/04/16 Pct Recovery = 91% Analysis Date = 10/04/16 Pct Recovery = 91% Analysis Date = 09/30/16 Pct Recovery = 91% Analysis Date = 09/30/16 Pct Recovery = 91% Analysis Date = 09/25/16 Pct Recovery = 91% Analysis Date = 09/25/16 Pct Recovery = 91% Analysis Date = 09/20/16 Pct Recovery = 91% Analysis Date = 09/20/16 Pct Recovery = 91% Analysis Date = 09/15/16 Pct Recovery = 91% Analysis Date = 09/15/16 Pct Recovery = 91% Analysis Date = 09/10/16 Pct Recovery = 91% Analysis Date = 09/10/16 Pct Recovery = 91% Analysis Date = 09/06/16 Pct Recovery = 91% Analysis Date = 09/06/16 Pct Recovery = 91% Analysis Date = 09/01/16 Pct Recovery = 91% Analysis Date = 09/01/16 Pct Recovery = 91% Analysis Date = 08/27/16 Pct Recovery = 91% Analysis Date = 08/27/16 Pct Recovery = 91% Analysis Date = 08/22/16 Pct Recovery = 91% Analysis Date = 08/22/16 Pct Recovery = 91% Analysis Date = 08/17/16 Pct Recovery = 91% Analysis Date = 08/17/16 Pct Recovery = 91% Analysis Date = 08/13/16 Pct Recovery = 91% Analysis Date = 08/13/16 Pct Recovery = 91% Analysis Date = 08/08/16 Pct Recovery = 91% Analysis Date = 08/08/16 Pct Recovery = 91% Analysis Date = 08/03/16 Pct Recovery = 90% Analysis Date = 08/03/16 Pct Recovery = 90% Analysis Date = 07/29/16 Pct Recovery = 90% Analysis Date = 07/29/16 Pct Recovery = 90% Analysis Date = 07/24/16 Pct Recovery = 90% Analysis Date = 07/24/16 Pct Recovery = 90% Analysis Date = 07/20/16 Pct Recovery = 90% Analysis Date = 07/20/16 Pct Recovery = 90% Analysis Date = 07/15/16 Pct Recovery = 90% Analysis Date = 07/15/16 Pct Recovery = 90% Analysis Date = 07/10/16 Pct Recovery = 90% Analysis Date = 07/10/16 Pct Recovery = 90% Analysis Date = 07/05/16 Pct Recovery = 90% Analysis Date = 07/05/16 Pct Recovery = 90% Analysis Date = 06/30/16 Pct Recovery = 90% Analysis Date = 06/30/16 Pct Recovery = 90% Analysis Date = 06/26/16 Pct Recovery = 90% Analysis Date = 06/26/16 Pct Recovery = 90% Analysis Date = 06/21/16 Pct Recovery = 90% Analysis Date = 06/21/16 Pct Recovery = 90% Analysis Date = 06/16/16 Pct Recovery = 90% Analysis Date = 06/16/16 Pct Recovery = 90% Analysis Date = 06/11/16 Pct Recovery = 90% Analysis Date = 06/11/16 Pct Recovery = 90% Analysis Date = 06/06/16 Pct Recovery = 90% Analysis Date = 06/06/16 Pct Recovery = 90% Analysis Date = 06/02/16 Pct Recovery = 90% Analysis Date = 06/02/16 Pct Recovery = 90% Analysis Date = 05/28/16 Pct Recovery = 90% Analysis Date = 05/28/16 Pct Recovery = 90% Analysis Date = 05/23/16 Pct Recovery = 90% Analysis Date = 05/23/16 Pct Recovery = 90% Analysis Date = 05/18/16 Pct Recovery = 90% Analysis Date = 05/18/16 Pct Recovery = 90% Analysis Date = 05/13/16 Pct Recovery = 90% Analysis Date = 05/13/16 Pct Recovery = 90% Analysis Date = 05/09/16 Pct Recovery = 90% Analysis Date = 05/09/16 Pct Recovery = 90% Analysis Date = 05/04/16 Pct Recovery = 90% Analysis Date = 05/04/16 Pct Recovery = 90% Analysis Date = 04/29/16 Pct Recovery = 90% Analysis Date = 04/29/16 Pct Recovery = 90% Analysis Date = 04/24/16 Pct Recovery = 90% Analysis Date = 04/24/16 Pct Recovery = 90% Analysis Date = 04/19/16 Pct Recovery = 90% Analysis Date = 04/19/16 Pct Recovery = 90% Analysis Date = 04/15/16 Pct Recovery = 90% Analysis Date = 04/15/16 Pct Recovery = 90% Analysis Date = 04/10/16 Pct Recovery = 90% Analysis Date = 04/10/16 Pct Recovery = 90% Analysis Date = 04/05/16 Pct Recovery = 90% Analysis Date = 04/05/16 Pct Recovery = 90% Analysis Date = 03/31/16 Pct Recovery = 90% Analysis Date = 03/31/16 Pct Recovery = 90% Analysis Date = 03/26/16 Pct Recovery = 89% Analysis Date = 03/26/16 Pct Recovery = 89% Analysis Date = 03/22/16 Pct Recovery = 89% Analysis Date = 03/22/16 Pct Recovery = 89% Analysis Date = 03/17/16 Pct Recovery = 89% Analysis Date = 03/17/16 Pct Recovery = 89% Analysis Date = 03/12/16 Pct Recovery = 89% Analysis Date = 03/12/16 Pct Recovery = 89% Analysis Date = 03/07/16 Pct Recovery = 89% Analysis Date = 03/07/16 Pct Recovery = 89% Analysis Date = 03/02/16 Pct Recovery = 89% Analysis Date = 03/02/16 Pct Recovery = 89% Analysis Date = 02/27/16 Pct Recovery = 89% Analysis Date = 02/27/16 Pct Recovery = 89% Analysis Date = 02/22/16 Pct Recovery = 89% Analysis Date = 02/22/16 Pct Recovery = 89% Analysis Date = 02/17/16 Pct Recovery = 89% Analysis Date = 02/17/16 Pct Recovery = 89% Analysis Date = 02/12/16 Pct Recovery = 89% Analysis Date = 02/12/16 Pct Recovery = 89% Analysis Date = 02/07/16 Pct Recovery = 89% Analysis Date = 02/07/16 Pct Recovery = 89% Analysis Date = 02/03/16 Pct Recovery = 89% Analysis Date = 02/03/16 Pct Recovery = 89% Analysis Date = 01/29/16 Pct Recovery = 89% Analysis Date = 01/29/16 Pct Recovery = 89% Analysis Date = 01/24/16 Pct Recovery = 89% Analysis Date = 01/24/16 Pct Recovery = 89% Analysis Date = 01/19/16 Pct Recovery = 89% Analysis Date = 01/19/16 Pct Recovery = 89% Analysis Date = 01/14/16 Pct Recovery = 88% Analysis Date = 01/14/16 Pct Recovery = 88% Analysis Date = 01/10/16 Pct Recovery = 88% Analysis Date = 01/10/16 Pct Recovery = 88% Analysis Date = 01/05/16 Pct Recovery = 88% Analysis Date = 01/05/16 Pct Recovery = 88% Analysis Date = 12/31/15 Pct Recovery = 88% Analysis Date = 12/31/15 Pct Recovery = 88% Analysis Date = 12/26/15 Pct Recovery = 88% Analysis Date = 12/26/15 Pct Recovery = 88% Analysis Date = 12/21/15 Pct Recovery = 88% Analysis Date = 12/21/15 Pct Recovery = 88% Analysis Date = 12/17/15 Pct Recovery = 88% Analysis Date = 12/17/15 Pct Recovery = 88% Analysis Date = 12/12/15 Pct Recovery = 88% Analysis Date = 12/12/15 Pct Recovery = 88% Analysis Date = 12/07/15 Pct Recovery = 88% Analysis Date = 12/07/15 Pct Recovery = 88% Analysis Date = 12/02/15 Pct Recovery = 88% Analysis Date = 12/02/15 Pct Recovery = 88% Analysis Date = 11/27/15 Pct Recovery = 88% Analysis Date = 11/27/15 Pct Recovery = 88% Analysis Date = 11/23/15 Pct Recovery = 88% Analysis Date = 11/23/15 Pct Recovery = 88% Analysis Date = 11/18/15 Pct Recovery = 88% Analysis Date = 11/18/15 Pct Recovery = 88% Analysis Date = 11/13/15 Pct Recovery = 88% Analysis Date = 11/13/15 Pct Recovery = 88% Analysis Date = 11/08/15 Pct Recovery = 88% Analysis Date = 11/08/15 Pct Recovery = 88% Analysis Date = 11/03/15 Pct Recovery = 88% Analysis Date = 11/03/15 Pct Recovery = 88% Analysis Date = 10/30/15 Pct Recovery = 88% Analysis Date = 10/30/15 Pct Recovery = 88% Analysis Date = 10/25/15 Pct Recovery = 87% Analysis Date = 10/25/15 Pct Recovery = 87% Analysis Date = 10/20/15 Pct Recovery = 87% Analysis Date = 10/20/15 Pct Recovery = 87% Analysis Date = 10/15/15 Pct Recovery = 87% Analysis Date = 10/15/15 Pct Recovery = 87% Analysis Date = 10/10/15 Pct Recovery = 87% Analysis Date = 10/10/15 Pct Recovery = 87% Analysis Date = 10/06/15 Pct Recovery = 87% Analysis Date = 10/06/15 Pct Recovery = 87% Analysis Date = 10/01/15 Pct Recovery = 87% Analysis Date = 10/01/15 Pct Recovery = 87% Analysis Date = 09/26/15 Pct Recovery = 87% Analysis Date = 09/26/15 Pct Recovery = 87% Analysis Date = 09/21/15 Pct Recovery = 87% Analysis Date = 09/21/15 Pct Recovery = 87% Analysis Date = 09/16/15 Pct Recovery = 87% Analysis Date = 09/16/15 Pct Recovery = 87% Analysis Date = 09/12/15 Pct Recovery = 88% Analysis Date = 09/12/15 Pct Recovery = 88% Analysis Date = 09/07/15 Pct Recovery = 88% Analysis Date = 09/07/15 Pct Recovery = 88% Analysis Date = 09/02/15 Pct Recovery = 88% Analysis Date = 09/02/15 Pct Recovery = 88% Analysis Date = 08/28/15 Pct Recovery = 88% Analysis Date = 08/28/15 Pct Recovery = 88% Analysis Date = 08/23/15 Pct Recovery = 88% Analysis Date = 08/23/15 Pct Recovery = 88% Analysis Date = 08/19/15 Pct Recovery = 88% Analysis Date = 08/19/15 Pct Recovery = 88% Analysis Date = 08/14/15 Pct Recovery = 88% Analysis Date = 08/14/15 Pct Recovery = 88% Analysis Date = 08/09/15 Pct Recovery = 88% Analysis Date = 08/09/15 Pct Recovery = 88% Analysis Date = 08/04/15 Pct Recovery = 88% Analysis Date = 08/04/15 Pct Recovery = 88% Analysis Date = 07/30/15 Pct Recovery = 88% Analysis Date = 07/30/15 Pct Recovery = 88% Analysis Date = 07/26/15 Pct Recovery = 88% Analysis Date = 07/26/15 Pct Recovery = 88% Analysis Date = 07/21/15 Pct Recovery = 88% Analysis Date = 07/21/15 Pct Recovery = 88% Analysis Date = 07/16/15 Pct Recovery = 88% Analysis Date = 07/16/15 Pct Recovery = 88% Analysis Date = 07/11/15 Pct Recovery = 88% Analysis Date = 07/11/15 Pct Recovery = 88% Analysis Date = 07/06/15 Pct Recovery = 88% Analysis Date = 07/06/15 Pct Recovery = 88% Analysis Date = 07/02/15 Pct Recovery = 88% Analysis Date = 07/02/15 Pct Recovery = 88% Analysis Date = 06/27/15 Pct Recovery = 88% Analysis Date = 06/27/15 Pct Recovery = 88% Analysis Date = 06/22/15 Pct Recovery = 88% Analysis Date = 06/22/15 Pct Recovery = 88% Analysis Date = 06/17/15 Pct Recovery = 88% Analysis Date = 06/17/15 Pct Recovery = 88% Analysis Date = 06/12/15 Pct Recovery = 88% Analysis Date = 06/12/15 Pct Recovery = 88% Analysis Date = 06/08/15 Pct Recovery = 88% Analysis Date = 06/08/15 Pct Recovery = 88% Analysis Date = 06/03/15 Pct Recovery = 88% Analysis Date = 06/03/15 Pct Recovery = 88% Analysis Date = 05/29/15 Pct Recovery = 88% Analysis Date = 05/29/15 Pct Recovery = 88% Analysis Date = 05/24/15 Pct Recovery = 89% Analysis Date = 05/24/15 Pct Recovery = 89% Analysis Date = 05/19/15 Pct Recovery = 89% Analysis Date = 05/19/15 Pct Recovery = 89% Analysis Date = 05/15/15 Pct Recovery = 89% Analysis Date = 05/15/15 Pct Recovery = 89% Analysis Date = 05/10/15 Pct Recovery = 89% Analysis Date = 05/10/15 Pct Recovery = 89% Analysis Date = 05/05/15 Pct Recovery = 89% Analysis Date = 05/05/15 Pct Recovery = 89% Analysis Date = 04/30/15 Pct Recovery = 89% Analysis Date = 04/30/15 Pct Recovery = 89% Analysis Date = 04/25/15 Pct Recovery = 89% Analysis Date = 04/25/15 Pct Recovery = 89% Analysis Date = 04/21/15 Pct Recovery = 90% Analysis Date = 04/21/15 Pct Recovery = 90% Analysis Date = 04/16/15 Pct Recovery = 90% Analysis Date = 04/16/15 Pct Recovery = 90% Analysis Date = 04/11/15 Pct Recovery = 90% Analysis Date = 04/11/15 Pct Recovery = 90% Analysis Date = 04/06/15 Pct Recovery = 90% Analysis Date = 04/06/15 Pct Recovery = 90% Analysis Date = 04/01/15 Pct Recovery = 90% Analysis Date = 04/01/15 Pct Recovery = 90% Analysis Date = 03/28/15 Pct Recovery = 90% Analysis Date = 03/28/15 Pct Recovery = 90% Analysis Date = 03/23/15 Pct Recovery = 90% Analysis Date = 03/23/15 Pct Recovery = 90% Analysis Date = 03/18/15 Pct Recovery = 91% Analysis Date = 03/18/15 Pct Recovery = 91% Analysis Date = 03/13/15 Pct Recovery = 91% Analysis Date = 03/13/15 Pct Recovery = 91% Analysis Date = 03/08/15 Pct Recovery = 91% Analysis Date = 03/08/15 Pct Recovery = 91% Analysis Date = 03/04/15 Pct Recovery = 91% Analysis Date = 03/04/15 Pct Recovery = 91% Analysis Date = 02/27/15 Pct Recovery = 91% Analysis Date = 02/27/15 Pct Recovery = 91% Analysis Date = 02/22/15 Pct Recovery = 92% Analysis Date = 02/22/15 Pct Recovery = 92% Analysis Date = 02/17/15 Pct Recovery = 92% Analysis Date = 02/17/15 Pct Recovery = 92% Analysis Date = 02/12/15 Pct Recovery = 92% Analysis Date = 02/12/15 Pct Recovery = 92% Analysis Date = 02/08/15 Pct Recovery = 92% Analysis Date = 02/08/15 Pct Recovery = 92% Analysis Date = 02/03/15 Pct Recovery = 92% Analysis Date = 02/03/15 Pct Recovery = 92% Analysis Date = 01/29/15 Pct Recovery = 93% Analysis Date = 01/29/15 Pct Recovery = 93% Analysis Date = 01/24/15 Pct Recovery = 93% Analysis Date = 01/24/15 Pct Recovery = 93% Analysis Date = 01/19/15 Pct Recovery = 93% Analysis Date = 01/19/15 Pct Recovery = 93% Analysis Date = 01/15/15 Pct Recovery = 93% Analysis Date = 01/15/15 Pct Recovery = 93% Analysis Date = 01/10/15 Pct Recovery = 93% Analysis Date = 01/10/15 Pct Recovery = 93% Analysis Date = 01/05/15 Pct Recovery = 94% Analysis Date = 01/05/15 Pct Recovery = 94% Analysis Date = 12/31/14 Pct Recovery = 94% Analysis Date = 12/31/14 Pct Recovery = 94% Analysis Date = 12/26/14 Pct Recovery = 94% Analysis Date = 12/26/14 Pct Recovery = 94% Analysis Date = 12/22/14 Pct Recovery = 94% Analysis Date = 12/22/14 Pct Recovery = 94% Analysis Date = 12/17/14 Pct Recovery = 94% Analysis Date = 12/17/14 Pct Recovery = 94% Analysis Date = 12/12/14 Pct Recovery = 95% Analysis Date = 12/12/14 Pct Recovery = 95% Analysis Date = 12/07/14 Pct Recovery = 95% Analysis Date = 12/07/14 Pct Recovery = 95% Analysis Date = 12/02/14 Pct Recovery = 95% Analysis Date = 12/02/14 Pct Recovery = 95% Analysis Date = 11/28/14 Pct Recovery = 95% Analysis Date = 11/28/14 Pct Recovery = 95% Analysis Date = 11/23/14 Pct Recovery = 95% Analysis Date = 11/23/14 Pct Recovery = 95% Analysis Date = 11/18/14 Pct Recovery = 96% Analysis Date = 11/18/14 Pct Recovery = 96% Analysis Date = 11/13/14 Pct Recovery = 96% Analysis Date = 11/13/14 Pct Recovery = 96% Analysis Date = 11/08/14 Pct Recovery = 96% Analysis Date = 11/08/14 Pct Recovery = 96% Analysis Date = 11/04/14 Pct Recovery = 96% Analysis Date = 11/04/14 Pct Recovery = 96% Analysis Date = 10/30/14 Pct Recovery = 96% Analysis Date = 10/30/14 Pct Recovery = 96% Analysis Date = 10/25/14 Pct Recovery = 97% Analysis Date = 10/25/14 Pct Recovery = 97% Analysis Date = 10/20/14 Pct Recovery = 97% Analysis Date = 10/20/14 Pct Recovery = 97% Analysis Date = 10/15/14 Pct Recovery = 97% Analysis Date = 10/15/14 Pct Recovery = 97% Analysis Date = 10/11/14 Pct Recovery = 97% Analysis Date = 10/11/14 Pct Recovery = 97% Analysis Date = 10/06/14 Pct Recovery = 97% Analysis Date = 10/06/14 Pct Recovery = 97% Analysis Date = 10/01/14 Pct Recovery = 97% Analysis Date = 10/01/14 Pct Recovery = 97% Analysis Date = 09/26/14 Pct Recovery = 98% Analysis Date = 09/26/14 Pct Recovery = 98% Analysis Date = 09/21/14 Pct Recovery = 98% Analysis Date = 09/21/14 Pct Recovery = 98% Analysis Date = 09/17/14 Pct Recovery = 98% Analysis Date = 09/17/14 Pct Recovery = 98% Analysis Date = 09/12/14 Pct Recovery = 98% Analysis Date = 09/12/14 Pct Recovery = 98% Analysis Date = 09/07/14 Pct Recovery = 98% Analysis Date = 09/07/14 Pct Recovery = 98% Analysis Date = 09/02/14 Pct Recovery = 98% Analysis Date = 09/02/14 Pct Recovery = 98% Analysis Date = 08/28/14 Pct Recovery = 99% Analysis Date = 08/28/14 Pct Recovery = 99% Analysis Date = 08/24/14 Pct Recovery = 99% Analysis Date = 08/24/14 Pct Recovery = 99% Analysis Date = 08/19/14 Pct Recovery = 99% Analysis Date = 08/19/14 Pct Recovery = 99% Analysis Date = 08/14/14 Pct Recovery = 99% Analysis Date = 08/14/14 Pct Recovery = 99% Analysis Date = 08/09/14 Pct Recovery = 99% Analysis Date = 08/09/14 Pct Recovery = 99% Analysis Date = 08/04/14 Pct Recovery = 99% Analysis Date = 08/04/14 Pct Recovery = 99% Analysis Date = 07/31/14 Pct Recovery = 100% Analysis Date = 07/31/14 Pct Recovery = 100% Analysis Date = 07/26/14 Pct Recovery = 100% Analysis Date = 07/26/14 Pct Recovery = 100% Analysis Date = 07/21/14 Pct Recovery = 100% Analysis Date = 07/21/14 Pct Recovery = 100% Analysis Date = 07/16/14 Pct Recovery = 100% Analysis Date = 07/16/14 Pct Recovery = 100% Analysis Date = 07/11/14 Pct Recovery = 100% Analysis Date = 07/11/14 Pct Recovery = 100% Analysis Date = 07/07/14 Pct Recovery = 100% Analysis Date = 07/07/14 Pct Recovery = 100% Analysis Date = 07/02/14 Pct Recovery = 101% Analysis Date = 07/02/14 Pct Recovery = 101% Analysis Date = 06/27/14 Pct Recovery = 101% Analysis Date = 06/27/14 Pct Recovery = 101% Analysis Date = 06/22/14 Pct Recovery = 101% Analysis Date = 06/22/14 Pct Recovery = 101% Analysis Date = 06/17/14 Pct Recovery = 101% Analysis Date = 06/17/14 Pct Recovery = 101% Analysis Date = 06/13/14 Pct Recovery = 101% Analysis Date = 06/13/14 Pct Recovery = 101% Analysis Date = 06/08/14 Pct Recovery = 101% Analysis Date = 06/08/14 Pct Recovery = 101% Analysis Date = 06/03/14 Pct Recovery = 102% Analysis Date = 06/03/14 Pct Recovery = 102% Analysis Date = 05/29/14 Pct Recovery = 102% Analysis Date = 05/29/14 Pct Recovery = 102% Analysis Date = 05/24/14 Pct Recovery = 102% Analysis Date = 05/24/14 Pct Recovery = 102% Analysis Date = 05/20/14 Pct Recovery = 102% Analysis Date = 05/20/14 Pct Recovery = 102% Analysis Date = 05/15/14 Pct Recovery = 102% Analysis Date = 05/15/14 Pct Recovery = 102% Analysis Date = 05/10/14 Pct Recovery = 103% Analysis Date = 05/10/14 Pct Recovery = 103% Analysis Date = 05/05/14 Pct Recovery = 103% Analysis Date = 05/05/14 Pct Recovery = 103% Analysis Date = 05/01/14 Pct Recovery = 103% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
VINYL CHLORIDE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 47 92% 15% 92% 15%
Total 47 92% 15% 92% 15%

Sample Statistics
VINYL CHLORIDE

Characteristic N % % Basis
Plotted 47 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 47 .  
False Negatives 0 0% 0 out of 47
Not Spiked 26 .  
False Positives 0 0% 0 out of 26