BQS OBSP Determination:
1,1-DICHLORO-2-PROPANONE
METHOD: 4437 , TESTIDCODE: 80336GM016
Open Data Set

 Analysis Date = 08/11/16 
 SpikeMix = Phenova B20160303: 25 µl & Supelco LC20145V: 25 µl & NSI 041416HVOC: 25 µl 
 Pct Recovery = 88%  Analysis Date = 01/10/15 
 SpikeMix = Abs 032014: 20 µl & ERA 0321-14-05A: 20 µl 
 Pct Recovery = 102%  Analysis Date = 08/13/14 
 SpikeMix = ERA 0321-14-05: 20 µl & Accu 214031128: 20 µl 
 Pct Recovery = 98%  Analysis Date = 07/11/14 
 SpikeMix = ChemService 2615700: 20 µl & Accu 214031128: 20 µl 
 Pct Recovery = 94%  Analysis Date = 07/03/14 
 SpikeMix = Abs 032014: 20 µl & ChemService 2615700: 20 µl 
 Pct Recovery = 92%  Analysis Date = 06/07/14 
 SpikeMix = ChemService 2615700: 20 µl & Supelco LC06437: 20 µl 
 Pct Recovery = 127%  Analysis Date = 06/06/14 
 SpikeMix = NSI 031814: 20 µl & ChemService 2615700: 20 µl 
 Pct Recovery = 122%  Analysis Date = 06/26/15 
 SpikeMix = ChemService 3818700: 25 µl & Accu 215041338: 25 µl 
 Pct Recovery = 95%  Analysis Date = 06/25/15 
 SpikeMix = ChemService 3818700: 25 µl & NSI 050515HVOC: 25 µl 
 Pct Recovery = 90%  Analysis Date = 01/22/16 
 SpikeMix = NSI 050515HVOC: 25 µl & ERA 0601-15-05: 25 µl 
 Pct Recovery = 98%  Analysis Date = 10/09/15 
 SpikeMix = ERA 0601-15-05: 25 µl & Accu 215041338: 25 µl 
 Pct Recovery = 92%  Analysis Date = 07/06/16 
 SpikeMix = Phenova B20160303: 15 µl & Accu 216041354: 15 µl & NSI 041416HVOC: 15 µl 
 Pct Recovery = 82%  Analysis Date = 06/03/16 
 SpikeMix = NSI 041516: 15 µl & Phenova B20160303: 15 µl & NSI 041416HVOC: 15 µl 
 Pct Recovery = 93%  Analysis Date = 04/28/16 
 SpikeMix = ChemService 3818700: 15 µl & Supelco LC13544: 15 µl 
 Pct Recovery = 102%  Analysis Date = 06/16/15 
 SpikeMix = ChemService 3818700: 15 µl & NSI 050515HVOC: 15 µl 
 Pct Recovery = 93%  Analysis Date = 05/14/15 
 SpikeMix = ChemService 3818700: 15 µl & Supelco LC13544: 15 µl 
 Pct Recovery = 97%  Analysis Date = 09/24/15 
 SpikeMix = Abs 040315: 15 µl & ERA 0601-15-05: 15 µl 
 Pct Recovery = 85%  Analysis Date = 08/24/15 
 SpikeMix = ERA 0601-15-05: 15 µl & Supelco LC13544: 15 µl 
 Pct Recovery = 86%  Analysis Date = 04/25/15 
 SpikeMix = Abs 032014: 10 µl & ERA 0321-14-05A: 10 µl 
 Pct Recovery = 104%  Analysis Date = 10/21/14 
 SpikeMix = ERA 0321-14-05A: 10 µl & Accu 214031128: 10 µl 
 Pct Recovery = 128%  Analysis Date = 09/06/14 
 SpikeMix = ERA 0321-14-05: 10 µl & Supelco LC06437: 10 µl 
 Pct Recovery = 109%  Analysis Date = 11/22/14 
 SpikeMix = ChemService 2615700: 10 µl & Supelco LC06437: 10 µl 
 Pct Recovery = 92%  Analysis Date = 07/30/14 
 SpikeMix = NSI 031814: 10 µl & ChemService 2615700: 10 µl 
 Pct Recovery = 94%  Analysis Date = 05/20/14 
 SpikeMix = ChemService 2615700: 10 µl & Accu 214031128: 10 µl 
 Pct Recovery = 89%  Analysis Date = 04/09/16 
 SpikeMix = Abs 040315: 10 µl & ChemService 3818700: 10 µl 
 Pct Recovery = 91%  Analysis Date = 12/10/15 
 SpikeMix = ChemService 3818700: 10 µl & Supelco LC13544: 10 µl 
 Pct Recovery = 112%  Analysis Date = 10/23/15 
 SpikeMix = Abs 040315: 10 µl & ChemService 3818700: 10 µl 
 Pct Recovery = 110%  Analysis Date = 05/20/15 
 SpikeMix = ChemService 3818700: 10 µl & Accu 215041338: 10 µl 
 Pct Recovery = 121%  Analysis Date = 02/12/16 
 SpikeMix = ERA 0601-15-05: 10 µl & Accu 215041338: 10 µl 
 Pct Recovery = 86%  Analysis Date = 12/05/15 
 SpikeMix = NSI 050515HVOC: 10 µl & ERA 0601-15-05: 10 µl 
 Pct Recovery = 91%  Analysis Date = 11/14/15 
 SpikeMix = ERA 0601-15-05: 10 µl 
 Pct Recovery = 89%  Analysis Date = 08/14/15 
 SpikeMix = Abs 040315: 10 µl & ERA 0601-15-05: 10 µl 
 Pct Recovery = 89%  Analysis Date = 08/10/16 
 Pct Recovery = 89%  Analysis Date = 08/06/16 
 Pct Recovery = 89%  Analysis Date = 08/06/16 
 Pct Recovery = 89%  Analysis Date = 08/02/16 
 Pct Recovery = 89%  Analysis Date = 08/02/16 
 Pct Recovery = 89%  Analysis Date = 07/29/16 
 Pct Recovery = 89%  Analysis Date = 07/29/16 
 Pct Recovery = 89%  Analysis Date = 07/25/16 
 Pct Recovery = 89%  Analysis Date = 07/25/16 
 Pct Recovery = 89%  Analysis Date = 07/21/16 
 Pct Recovery = 90%  Analysis Date = 07/21/16 
 Pct Recovery = 90%  Analysis Date = 07/17/16 
 Pct Recovery = 90%  Analysis Date = 07/17/16 
 Pct Recovery = 90%  Analysis Date = 07/13/16 
 Pct Recovery = 90%  Analysis Date = 07/13/16 
 Pct Recovery = 90%  Analysis Date = 07/09/16 
 Pct Recovery = 90%  Analysis Date = 07/09/16 
 Pct Recovery = 90%  Analysis Date = 07/05/16 
 Pct Recovery = 90%  Analysis Date = 07/05/16 
 Pct Recovery = 90%  Analysis Date = 07/01/16 
 Pct Recovery = 90%  Analysis Date = 07/01/16 
 Pct Recovery = 90%  Analysis Date = 06/27/16 
 Pct Recovery = 90%  Analysis Date = 06/27/16 
 Pct Recovery = 90%  Analysis Date = 06/23/16 
 Pct Recovery = 90%  Analysis Date = 06/23/16 
 Pct Recovery = 90%  Analysis Date = 06/19/16 
 Pct Recovery = 91%  Analysis Date = 06/19/16 
 Pct Recovery = 91%  Analysis Date = 06/15/16 
 Pct Recovery = 91%  Analysis Date = 06/15/16 
 Pct Recovery = 91%  Analysis Date = 06/10/16 
 Pct Recovery = 91%  Analysis Date = 06/10/16 
 Pct Recovery = 91%  Analysis Date = 06/06/16 
 Pct Recovery = 91%  Analysis Date = 06/06/16 
 Pct Recovery = 91%  Analysis Date = 06/02/16 
 Pct Recovery = 91%  Analysis Date = 06/02/16 
 Pct Recovery = 91%  Analysis Date = 05/29/16 
 Pct Recovery = 91%  Analysis Date = 05/29/16 
 Pct Recovery = 91%  Analysis Date = 05/25/16 
 Pct Recovery = 91%  Analysis Date = 05/25/16 
 Pct Recovery = 91%  Analysis Date = 05/21/16 
 Pct Recovery = 91%  Analysis Date = 05/21/16 
 Pct Recovery = 91%  Analysis Date = 05/17/16 
 Pct Recovery = 91%  Analysis Date = 05/17/16 
 Pct Recovery = 91%  Analysis Date = 05/13/16 
 Pct Recovery = 91%  Analysis Date = 05/13/16 
 Pct Recovery = 91%  Analysis Date = 05/09/16 
 Pct Recovery = 92%  Analysis Date = 05/09/16 
 Pct Recovery = 92%  Analysis Date = 05/05/16 
 Pct Recovery = 92%  Analysis Date = 05/05/16 
 Pct Recovery = 92%  Analysis Date = 05/01/16 
 Pct Recovery = 92%  Analysis Date = 05/01/16 
 Pct Recovery = 92%  Analysis Date = 04/27/16 
 Pct Recovery = 92%  Analysis Date = 04/27/16 
 Pct Recovery = 92%  Analysis Date = 04/23/16 
 Pct Recovery = 92%  Analysis Date = 04/23/16 
 Pct Recovery = 92%  Analysis Date = 04/19/16 
 Pct Recovery = 92%  Analysis Date = 04/19/16 
 Pct Recovery = 92%  Analysis Date = 04/14/16 
 Pct Recovery = 92%  Analysis Date = 04/14/16 
 Pct Recovery = 92%  Analysis Date = 04/10/16 
 Pct Recovery = 92%  Analysis Date = 04/10/16 
 Pct Recovery = 92%  Analysis Date = 04/06/16 
 Pct Recovery = 92%  Analysis Date = 04/06/16 
 Pct Recovery = 92%  Analysis Date = 04/02/16 
 Pct Recovery = 93%  Analysis Date = 04/02/16 
 Pct Recovery = 93%  Analysis Date = 03/29/16 
 Pct Recovery = 93%  Analysis Date = 03/29/16 
 Pct Recovery = 93%  Analysis Date = 03/25/16 
 Pct Recovery = 93%  Analysis Date = 03/25/16 
 Pct Recovery = 93%  Analysis Date = 03/21/16 
 Pct Recovery = 93%  Analysis Date = 03/21/16 
 Pct Recovery = 93%  Analysis Date = 03/17/16 
 Pct Recovery = 93%  Analysis Date = 03/17/16 
 Pct Recovery = 93%  Analysis Date = 03/13/16 
 Pct Recovery = 93%  Analysis Date = 03/13/16 
 Pct Recovery = 93%  Analysis Date = 03/09/16 
 Pct Recovery = 93%  Analysis Date = 03/09/16 
 Pct Recovery = 93%  Analysis Date = 03/05/16 
 Pct Recovery = 93%  Analysis Date = 03/05/16 
 Pct Recovery = 93%  Analysis Date = 03/01/16 
 Pct Recovery = 93%  Analysis Date = 03/01/16 
 Pct Recovery = 93%  Analysis Date = 02/26/16 
 Pct Recovery = 93%  Analysis Date = 02/26/16 
 Pct Recovery = 93%  Analysis Date = 02/22/16 
 Pct Recovery = 94%  Analysis Date = 02/22/16 
 Pct Recovery = 94%  Analysis Date = 02/17/16 
 Pct Recovery = 94%  Analysis Date = 02/17/16 
 Pct Recovery = 94%  Analysis Date = 02/13/16 
 Pct Recovery = 94%  Analysis Date = 02/13/16 
 Pct Recovery = 94%  Analysis Date = 02/09/16 
 Pct Recovery = 94%  Analysis Date = 02/09/16 
 Pct Recovery = 94%  Analysis Date = 02/05/16 
 Pct Recovery = 94%  Analysis Date = 02/05/16 
 Pct Recovery = 94%  Analysis Date = 02/01/16 
 Pct Recovery = 94%  Analysis Date = 02/01/16 
 Pct Recovery = 94%  Analysis Date = 01/28/16 
 Pct Recovery = 94%  Analysis Date = 01/28/16 
 Pct Recovery = 94%  Analysis Date = 01/24/16 
 Pct Recovery = 94%  Analysis Date = 01/24/16 
 Pct Recovery = 94%  Analysis Date = 01/20/16 
 Pct Recovery = 94%  Analysis Date = 01/20/16 
 Pct Recovery = 94%  Analysis Date = 01/16/16 
 Pct Recovery = 94%  Analysis Date = 01/16/16 
 Pct Recovery = 94%  Analysis Date = 01/12/16 
 Pct Recovery = 94%  Analysis Date = 01/12/16 
 Pct Recovery = 94%  Analysis Date = 01/08/16 
 Pct Recovery = 94%  Analysis Date = 01/08/16 
 Pct Recovery = 94%  Analysis Date = 01/04/16 
 Pct Recovery = 94%  Analysis Date = 01/04/16 
 Pct Recovery = 94%  Analysis Date = 12/31/15 
 Pct Recovery = 94%  Analysis Date = 12/31/15 
 Pct Recovery = 94%  Analysis Date = 12/27/15 
 Pct Recovery = 95%  Analysis Date = 12/27/15 
 Pct Recovery = 95%  Analysis Date = 12/23/15 
 Pct Recovery = 95%  Analysis Date = 12/23/15 
 Pct Recovery = 95%  Analysis Date = 12/18/15 
 Pct Recovery = 95%  Analysis Date = 12/18/15 
 Pct Recovery = 95%  Analysis Date = 12/14/15 
 Pct Recovery = 95%  Analysis Date = 12/14/15 
 Pct Recovery = 95%  Analysis Date = 12/10/15 
 Pct Recovery = 95%  Analysis Date = 12/10/15 
 Pct Recovery = 95%  Analysis Date = 12/06/15 
 Pct Recovery = 95%  Analysis Date = 12/06/15 
 Pct Recovery = 95%  Analysis Date = 12/02/15 
 Pct Recovery = 95%  Analysis Date = 12/02/15 
 Pct Recovery = 95%  Analysis Date = 11/28/15 
 Pct Recovery = 95%  Analysis Date = 11/28/15 
 Pct Recovery = 95%  Analysis Date = 11/24/15 
 Pct Recovery = 95%  Analysis Date = 11/24/15 
 Pct Recovery = 95%  Analysis Date = 11/20/15 
 Pct Recovery = 95%  Analysis Date = 11/20/15 
 Pct Recovery = 95%  Analysis Date = 11/16/15 
 Pct Recovery = 95%  Analysis Date = 11/16/15 
 Pct Recovery = 95%  Analysis Date = 11/12/15 
 Pct Recovery = 95%  Analysis Date = 11/12/15 
 Pct Recovery = 95%  Analysis Date = 11/08/15 
 Pct Recovery = 95%  Analysis Date = 11/08/15 
 Pct Recovery = 95%  Analysis Date = 11/04/15 
 Pct Recovery = 95%  Analysis Date = 11/04/15 
 Pct Recovery = 95%  Analysis Date = 10/31/15 
 Pct Recovery = 95%  Analysis Date = 10/31/15 
 Pct Recovery = 95%  Analysis Date = 10/27/15 
 Pct Recovery = 95%  Analysis Date = 10/27/15 
 Pct Recovery = 95%  Analysis Date = 10/22/15 
 Pct Recovery = 95%  Analysis Date = 10/22/15 
 Pct Recovery = 95%  Analysis Date = 10/18/15 
 Pct Recovery = 95%  Analysis Date = 10/18/15 
 Pct Recovery = 95%  Analysis Date = 10/14/15 
 Pct Recovery = 95%  Analysis Date = 10/14/15 
 Pct Recovery = 95%  Analysis Date = 10/10/15 
 Pct Recovery = 95%  Analysis Date = 10/10/15 
 Pct Recovery = 95%  Analysis Date = 10/06/15 
 Pct Recovery = 95%  Analysis Date = 10/06/15 
 Pct Recovery = 95%  Analysis Date = 10/02/15 
 Pct Recovery = 95%  Analysis Date = 10/02/15 
 Pct Recovery = 95%  Analysis Date = 09/28/15 
 Pct Recovery = 95%  Analysis Date = 09/28/15 
 Pct Recovery = 95%  Analysis Date = 09/24/15 
 Pct Recovery = 95%  Analysis Date = 09/24/15 
 Pct Recovery = 95%  Analysis Date = 09/20/15 
 Pct Recovery = 95%  Analysis Date = 09/20/15 
 Pct Recovery = 95%  Analysis Date = 09/16/15 
 Pct Recovery = 95%  Analysis Date = 09/16/15 
 Pct Recovery = 95%  Analysis Date = 09/12/15 
 Pct Recovery = 96%  Analysis Date = 09/12/15 
 Pct Recovery = 96%  Analysis Date = 09/08/15 
 Pct Recovery = 96%  Analysis Date = 09/08/15 
 Pct Recovery = 96%  Analysis Date = 09/04/15 
 Pct Recovery = 96%  Analysis Date = 09/04/15 
 Pct Recovery = 96%  Analysis Date = 08/31/15 
 Pct Recovery = 96%  Analysis Date = 08/31/15 
 Pct Recovery = 96%  Analysis Date = 08/26/15 
 Pct Recovery = 96%  Analysis Date = 08/26/15 
 Pct Recovery = 96%  Analysis Date = 08/22/15 
 Pct Recovery = 96%  Analysis Date = 08/22/15 
 Pct Recovery = 96%  Analysis Date = 08/18/15 
 Pct Recovery = 96%  Analysis Date = 08/18/15 
 Pct Recovery = 96%  Analysis Date = 08/14/15 
 Pct Recovery = 96%  Analysis Date = 08/14/15 
 Pct Recovery = 96%  Analysis Date = 08/10/15 
 Pct Recovery = 96%  Analysis Date = 08/10/15 
 Pct Recovery = 96%  Analysis Date = 08/06/15 
 Pct Recovery = 96%  Analysis Date = 08/06/15 
 Pct Recovery = 96%  Analysis Date = 08/02/15 
 Pct Recovery = 97%  Analysis Date = 08/02/15 
 Pct Recovery = 97%  Analysis Date = 07/29/15 
 Pct Recovery = 97%  Analysis Date = 07/29/15 
 Pct Recovery = 97%  Analysis Date = 07/25/15 
 Pct Recovery = 97%  Analysis Date = 07/25/15 
 Pct Recovery = 97%  Analysis Date = 07/21/15 
 Pct Recovery = 97%  Analysis Date = 07/21/15 
 Pct Recovery = 97%  Analysis Date = 07/17/15 
 Pct Recovery = 97%  Analysis Date = 07/17/15 
 Pct Recovery = 97%  Analysis Date = 07/13/15 
 Pct Recovery = 97%  Analysis Date = 07/13/15 
 Pct Recovery = 97%  Analysis Date = 07/09/15 
 Pct Recovery = 97%  Analysis Date = 07/09/15 
 Pct Recovery = 97%  Analysis Date = 07/05/15 
 Pct Recovery = 97%  Analysis Date = 07/05/15 
 Pct Recovery = 97%  Analysis Date = 06/30/15 
 Pct Recovery = 97%  Analysis Date = 06/30/15 
 Pct Recovery = 97%  Analysis Date = 06/26/15 
 Pct Recovery = 97%  Analysis Date = 06/26/15 
 Pct Recovery = 97%  Analysis Date = 06/22/15 
 Pct Recovery = 98%  Analysis Date = 06/22/15 
 Pct Recovery = 98%  Analysis Date = 06/18/15 
 Pct Recovery = 98%  Analysis Date = 06/18/15 
 Pct Recovery = 98%  Analysis Date = 06/14/15 
 Pct Recovery = 98%  Analysis Date = 06/14/15 
 Pct Recovery = 98%  Analysis Date = 06/10/15 
 Pct Recovery = 98%  Analysis Date = 06/10/15 
 Pct Recovery = 98%  Analysis Date = 06/06/15 
 Pct Recovery = 98%  Analysis Date = 06/06/15 
 Pct Recovery = 98%  Analysis Date = 06/02/15 
 Pct Recovery = 98%  Analysis Date = 06/02/15 
 Pct Recovery = 98%  Analysis Date = 05/29/15 
 Pct Recovery = 98%  Analysis Date = 05/29/15 
 Pct Recovery = 98%  Analysis Date = 05/25/15 
 Pct Recovery = 98%  Analysis Date = 05/25/15 
 Pct Recovery = 98%  Analysis Date = 05/21/15 
 Pct Recovery = 98%  Analysis Date = 05/21/15 
 Pct Recovery = 98%  Analysis Date = 05/17/15 
 Pct Recovery = 99%  Analysis Date = 05/17/15 
 Pct Recovery = 99%  Analysis Date = 05/13/15 
 Pct Recovery = 99%  Analysis Date = 05/13/15 
 Pct Recovery = 99%  Analysis Date = 05/09/15 
 Pct Recovery = 99%  Analysis Date = 05/09/15 
 Pct Recovery = 99%  Analysis Date = 05/05/15 
 Pct Recovery = 99%  Analysis Date = 05/05/15 
 Pct Recovery = 99%  Analysis Date = 04/30/15 
 Pct Recovery = 99%  Analysis Date = 04/30/15 
 Pct Recovery = 99%  Analysis Date = 04/26/15 
 Pct Recovery = 100%  Analysis Date = 04/26/15 
 Pct Recovery = 100%  Analysis Date = 04/22/15 
 Pct Recovery = 100%  Analysis Date = 04/22/15 
 Pct Recovery = 100%  Analysis Date = 04/18/15 
 Pct Recovery = 100%  Analysis Date = 04/18/15 
 Pct Recovery = 100%  Analysis Date = 04/14/15 
 Pct Recovery = 100%  Analysis Date = 04/14/15 
 Pct Recovery = 100%  Analysis Date = 04/10/15 
 Pct Recovery = 100%  Analysis Date = 04/10/15 
 Pct Recovery = 100%  Analysis Date = 04/06/15 
 Pct Recovery = 100%  Analysis Date = 04/06/15 
 Pct Recovery = 100%  Analysis Date = 04/02/15 
 Pct Recovery = 100%  Analysis Date = 04/02/15 
 Pct Recovery = 100%  Analysis Date = 03/29/15 
 Pct Recovery = 100%  Analysis Date = 03/29/15 
 Pct Recovery = 100%  Analysis Date = 03/25/15 
 Pct Recovery = 100%  Analysis Date = 03/25/15 
 Pct Recovery = 100%  Analysis Date = 03/21/15 
 Pct Recovery = 101%  Analysis Date = 03/21/15 
 Pct Recovery = 101%  Analysis Date = 03/17/15 
 Pct Recovery = 101%  Analysis Date = 03/17/15 
 Pct Recovery = 101%  Analysis Date = 03/13/15 
 Pct Recovery = 101%  Analysis Date = 03/13/15 
 Pct Recovery = 101%  Analysis Date = 03/09/15 
 Pct Recovery = 101%  Analysis Date = 03/09/15 
 Pct Recovery = 101%  Analysis Date = 03/04/15 
 Pct Recovery = 101%  Analysis Date = 03/04/15 
 Pct Recovery = 101%  Analysis Date = 02/28/15 
 Pct Recovery = 101%  Analysis Date = 02/28/15 
 Pct Recovery = 101%  Analysis Date = 02/24/15 
 Pct Recovery = 101%  Analysis Date = 02/24/15 
 Pct Recovery = 101%  Analysis Date = 02/20/15 
 Pct Recovery = 101%  Analysis Date = 02/20/15 
 Pct Recovery = 101%  Analysis Date = 02/16/15 
 Pct Recovery = 101%  Analysis Date = 02/16/15 
 Pct Recovery = 101%  Analysis Date = 02/12/15 
 Pct Recovery = 102%  Analysis Date = 02/12/15 
 Pct Recovery = 102%  Analysis Date = 02/08/15 
 Pct Recovery = 102%  Analysis Date = 02/08/15 
 Pct Recovery = 102%  Analysis Date = 02/04/15 
 Pct Recovery = 102%  Analysis Date = 02/04/15 
 Pct Recovery = 102%  Analysis Date = 01/31/15 
 Pct Recovery = 102%  Analysis Date = 01/31/15 
 Pct Recovery = 102%  Analysis Date = 01/27/15 
 Pct Recovery = 102%  Analysis Date = 01/27/15 
 Pct Recovery = 102%  Analysis Date = 01/23/15 
 Pct Recovery = 102%  Analysis Date = 01/23/15 
 Pct Recovery = 102%  Analysis Date = 01/19/15 
 Pct Recovery = 102%  Analysis Date = 01/19/15 
 Pct Recovery = 102%  Analysis Date = 01/15/15 
 Pct Recovery = 102%  Analysis Date = 01/15/15 
 Pct Recovery = 102%  Analysis Date = 01/11/15 
 Pct Recovery = 102%  Analysis Date = 01/11/15 
 Pct Recovery = 102%  Analysis Date = 01/06/15 
 Pct Recovery = 102%  Analysis Date = 01/06/15 
 Pct Recovery = 102%  Analysis Date = 01/02/15 
 Pct Recovery = 103%  Analysis Date = 01/02/15 
 Pct Recovery = 103%  Analysis Date = 12/29/14 
 Pct Recovery = 103%  Analysis Date = 12/29/14 
 Pct Recovery = 103%  Analysis Date = 12/25/14 
 Pct Recovery = 103%  Analysis Date = 12/25/14 
 Pct Recovery = 103%  Analysis Date = 12/21/14 
 Pct Recovery = 103%  Analysis Date = 12/21/14 
 Pct Recovery = 103%  Analysis Date = 12/17/14 
 Pct Recovery = 103%  Analysis Date = 12/17/14 
 Pct Recovery = 103%  Analysis Date = 12/13/14 
 Pct Recovery = 103%  Analysis Date = 12/13/14 
 Pct Recovery = 103%  Analysis Date = 12/09/14 
 Pct Recovery = 103%  Analysis Date = 12/09/14 
 Pct Recovery = 103%  Analysis Date = 12/05/14 
 Pct Recovery = 103%  Analysis Date = 12/05/14 
 Pct Recovery = 103%  Analysis Date = 12/01/14 
 Pct Recovery = 103%  Analysis Date = 12/01/14 
 Pct Recovery = 103%  Analysis Date = 11/27/14 
 Pct Recovery = 103%  Analysis Date = 11/27/14 
 Pct Recovery = 103%  Analysis Date = 11/23/14 
 Pct Recovery = 104%  Analysis Date = 11/23/14 
 Pct Recovery = 104%  Analysis Date = 11/19/14 
 Pct Recovery = 104%  Analysis Date = 11/19/14 
 Pct Recovery = 104%  Analysis Date = 11/15/14 
 Pct Recovery = 104%  Analysis Date = 11/15/14 
 Pct Recovery = 104%  Analysis Date = 11/11/14 
 Pct Recovery = 104%  Analysis Date = 11/11/14 
 Pct Recovery = 104%  Analysis Date = 11/06/14 
 Pct Recovery = 104%  Analysis Date = 11/06/14 
 Pct Recovery = 104%  Analysis Date = 11/02/14 
 Pct Recovery = 104%  Analysis Date = 11/02/14 
 Pct Recovery = 104%  Analysis Date = 10/29/14 
 Pct Recovery = 104%  Analysis Date = 10/29/14 
 Pct Recovery = 104%  Analysis Date = 10/25/14 
 Pct Recovery = 104%  Analysis Date = 10/25/14 
 Pct Recovery = 104%  Analysis Date = 10/21/14 
 Pct Recovery = 104%  Analysis Date = 10/21/14 
 Pct Recovery = 104%  Analysis Date = 10/17/14 
 Pct Recovery = 104%  Analysis Date = 10/17/14 
 Pct Recovery = 104%  Analysis Date = 10/13/14 
 Pct Recovery = 104%  Analysis Date = 10/13/14 
 Pct Recovery = 104%  Analysis Date = 10/09/14 
 Pct Recovery = 104%  Analysis Date = 10/09/14 
 Pct Recovery = 104%  Analysis Date = 10/05/14 
 Pct Recovery = 104%  Analysis Date = 10/05/14 
 Pct Recovery = 104%  Analysis Date = 10/01/14 
 Pct Recovery = 104%  Analysis Date = 10/01/14 
 Pct Recovery = 104%  Analysis Date = 09/27/14 
 Pct Recovery = 104%  Analysis Date = 09/27/14 
 Pct Recovery = 104%  Analysis Date = 09/23/14 
 Pct Recovery = 104%  Analysis Date = 09/23/14 
 Pct Recovery = 104%  Analysis Date = 09/19/14 
 Pct Recovery = 104%  Analysis Date = 09/19/14 
 Pct Recovery = 104%  Analysis Date = 09/15/14 
 Pct Recovery = 104%  Analysis Date = 09/15/14 
 Pct Recovery = 104%  Analysis Date = 09/10/14 
 Pct Recovery = 104%  Analysis Date = 09/10/14 
 Pct Recovery = 104%  Analysis Date = 09/06/14 
 Pct Recovery = 104%  Analysis Date = 09/06/14 
 Pct Recovery = 104%  Analysis Date = 09/02/14 
 Pct Recovery = 104%  Analysis Date = 09/02/14 
 Pct Recovery = 104%  Analysis Date = 08/29/14 
 Pct Recovery = 104%  Analysis Date = 08/29/14 
 Pct Recovery = 104%  Analysis Date = 08/25/14 
 Pct Recovery = 104%  Analysis Date = 08/25/14 
 Pct Recovery = 104%  Analysis Date = 08/21/14 
 Pct Recovery = 104%  Analysis Date = 08/21/14 
 Pct Recovery = 104%  Analysis Date = 08/17/14 
 Pct Recovery = 104%  Analysis Date = 08/17/14 
 Pct Recovery = 104%  Analysis Date = 08/13/14 
 Pct Recovery = 104%  Analysis Date = 08/13/14 
 Pct Recovery = 104%  Analysis Date = 08/09/14 
 Pct Recovery = 104%  Analysis Date = 08/09/14 
 Pct Recovery = 104%  Analysis Date = 08/05/14 
 Pct Recovery = 104%  Analysis Date = 08/05/14 
 Pct Recovery = 104%  Analysis Date = 08/01/14 
 Pct Recovery = 104%  Analysis Date = 08/01/14 
 Pct Recovery = 104%  Analysis Date = 07/28/14 
 Pct Recovery = 104%  Analysis Date = 07/28/14 
 Pct Recovery = 104%  Analysis Date = 07/24/14 
 Pct Recovery = 104%  Analysis Date = 07/24/14 
 Pct Recovery = 104%  Analysis Date = 07/20/14 
 Pct Recovery = 104%  Analysis Date = 07/20/14 
 Pct Recovery = 104%  Analysis Date = 07/15/14 
 Pct Recovery = 104%  Analysis Date = 07/15/14 
 Pct Recovery = 104%  Analysis Date = 07/11/14 
 Pct Recovery = 104%  Analysis Date = 07/11/14 
 Pct Recovery = 104%  Analysis Date = 07/07/14 
 Pct Recovery = 104%  Analysis Date = 07/07/14 
 Pct Recovery = 104%  Analysis Date = 07/03/14 
 Pct Recovery = 104%  Analysis Date = 07/03/14 
 Pct Recovery = 104%  Analysis Date = 06/29/14 
 Pct Recovery = 104%  Analysis Date = 06/29/14 
 Pct Recovery = 104%  Analysis Date = 06/25/14 
 Pct Recovery = 104%  Analysis Date = 06/25/14 
 Pct Recovery = 104%  Analysis Date = 06/21/14 
 Pct Recovery = 104%  Analysis Date = 06/21/14 
 Pct Recovery = 104%  Analysis Date = 06/17/14 
 Pct Recovery = 104%  Analysis Date = 06/17/14 
 Pct Recovery = 104%  Analysis Date = 06/13/14 
 Pct Recovery = 104%  Analysis Date = 06/13/14 
 Pct Recovery = 104%  Analysis Date = 06/09/14 
 Pct Recovery = 104%  Analysis Date = 06/09/14 
 Pct Recovery = 104%  Analysis Date = 06/05/14 
 Pct Recovery = 104%  Analysis Date = 06/05/14 
 Pct Recovery = 104%  Analysis Date = 06/01/14 
 Pct Recovery = 104%  Analysis Date = 06/01/14 
 Pct Recovery = 104%  Analysis Date = 05/28/14 
 Pct Recovery = 104%  Analysis Date = 05/28/14 
 Pct Recovery = 104%  Analysis Date = 05/24/14 
 Pct Recovery = 105%  Analysis Date = 05/24/14 
 Pct Recovery = 105%  Analysis Date = 05/20/14 
 Pct Recovery = 105%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
1,1-DICHLORO-2-PROPANONE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 32 98% 12% 93% 10%
Total 32 98% 12% 93% 10%

Sample Statistics
1,1-DICHLORO-2-PROPANONE

Characteristic N % % Basis
Plotted 32 100% Spiked
Estimated Values 2 6% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 32 .  
False Negatives 0 0% 0 out of 32
Not Spiked 23 .  
False Positives 0 0% 0 out of 23

BQS OBSP Determination:
1,2,3-TRICHLOROPROPANE
METHOD: 4437 , TESTIDCODE: 77443GM016
Open Data Set

 Analysis Date = 06/29/16 
 SpikeMix = NSI 041516: 40 µl & ChemService 5082800: 40 µl 
 Pct Recovery = 93%  Analysis Date = 08/13/14 
 SpikeMix = ERA 0321-14-05: 20 µl & Accu 214031128: 20 µl 
 Pct Recovery = 90%  Analysis Date = 07/23/14 
 SpikeMix = Accu 214031128: 20 µl & Abs 032014: 20 µl 
 Pct Recovery = 85%  Analysis Date = 07/11/14 
 SpikeMix = ChemService 2615700: 20 µl & Accu 214031128: 20 µl 
 Pct Recovery = 91%  Analysis Date = 05/07/14 
 SpikeMix = NSI 031814: 20 µl & Accu 214031128: 20 µl 
 Pct Recovery = 85%  Analysis Date = 07/14/16 
 SpikeMix = NSI 041516: 25 µl & ChemService 5082800: 25 µl & NSI 041416HVOC: 25 µl 
 Pct Recovery = 104%  Analysis Date = 01/22/16 
 SpikeMix = NSI 050515HVOC: 25 µl & ERA 0601-15-05: 25 µl 
 Pct Recovery = 100%  Analysis Date = 10/09/15 
 SpikeMix = Supelco LC13544: 25 µl & NSI 050515HVOC: 25 µl 
 Pct Recovery = 99%  Analysis Date = 06/25/15 
 SpikeMix = ChemService 3818700: 25 µl & NSI 050515HVOC: 25 µl 
 Pct Recovery = 99%  Analysis Date = 08/11/16 
 SpikeMix = Phenova B20160303: 25 µl & Supelco LC20145V: 25 µl & NSI 041416HVOC: 25 µl 
 Pct Recovery = 96%  Analysis Date = 03/19/15 
 SpikeMix = Supelco LC06437: 20 µl & NSI 031814: 20 µl 
 Pct Recovery = 88%  Analysis Date = 08/20/14 
 SpikeMix = Supelco LC06437: 20 µl & Abs 032014: 20 µl 
 Pct Recovery = 95%  Analysis Date = 06/07/14 
 SpikeMix = ChemService 2615700: 20 µl & Supelco LC06437: 20 µl 
 Pct Recovery = 98%  Analysis Date = 12/13/14 
 SpikeMix = Accu 214031128: 10 µl & NSI 031814: 10 µl 
 Pct Recovery = 92%  Analysis Date = 10/21/14 
 SpikeMix = ERA 0321-14-05A: 10 µl & Accu 214031128: 10 µl 
 Pct Recovery = 90%  Analysis Date = 09/11/14 
 SpikeMix = Accu 214031128: 10 µl & Abs 032014: 10 µl 
 Pct Recovery = 90%  Analysis Date = 05/20/14 
 SpikeMix = ChemService 2615700: 10 µl & Accu 214031128: 10 µl 
 Pct Recovery = 85%  Analysis Date = 07/27/16 
 SpikeMix = ChemService 5082800: 15 µl & Supelco LC20145V: 15 µl & Accu 216041225: 15 µl 
 Pct Recovery = 94%  Analysis Date = 06/23/16 
 SpikeMix = . 
 Pct Recovery = 107%  Analysis Date = 11/25/15 
 SpikeMix = Accu 215041338: 15 µl & Abs 040315: 15 µl 
 Pct Recovery = 91%  Analysis Date = 09/24/15 
 SpikeMix = Abs 040315: 15 µl & ERA 0601-15-05: 15 µl 
 Pct Recovery = 97%  Analysis Date = 09/05/15 
 SpikeMix = Accu 215041338: 15 µl & NSI 050515HVOC: 15 µl 
 Pct Recovery = 108%  Analysis Date = 07/30/15 
 SpikeMix = Supelco LC13544: 15 µl & NSI 050515HVOC: 15 µl 
 Pct Recovery = 109%  Analysis Date = 06/16/15 
 SpikeMix = ChemService 3818700: 15 µl & NSI 050515HVOC: 15 µl 
 Pct Recovery = 104%  Analysis Date = 07/06/16 
 SpikeMix = Phenova B20160303: 15 µl & Accu 216041354: 15 µl & NSI 041416HVOC: 15 µl 
 Pct Recovery = 98%  Analysis Date = 06/03/16 
 SpikeMix = NSI 041516: 15 µl & Phenova B20160303: 15 µl & NSI 041416HVOC: 15 µl 
 Pct Recovery = 117%  Analysis Date = 11/22/14 
 SpikeMix = ChemService 2615700: 10 µl & Supelco LC06437: 10 µl 
 Pct Recovery = 95%  Analysis Date = 09/06/14 
 SpikeMix = ERA 0321-14-05: 10 µl & Supelco LC06437: 10 µl 
 Pct Recovery = 92%  Analysis Date = 06/17/14 
 SpikeMix = Supelco LC06437: 10 µl & Abs 032014: 10 µl 
 Pct Recovery = 88%  Analysis Date = 04/09/16 
 SpikeMix = Abs 040315: 10 µl & ChemService 3818700: 10 µl 
 Pct Recovery = 93%  Analysis Date = 03/22/16 
 SpikeMix = Supelco LC13544: 10 µl & NSI 050515HVOC: 10 µl 
 Pct Recovery = 116%  Analysis Date = 01/05/16 
 SpikeMix = Accu 215041338: 10 µl & Abs 040315: 10 µl 
 Pct Recovery = 101%  Analysis Date = 12/05/15 
 SpikeMix = NSI 050515HVOC: 10 µl & ERA 0601-15-05: 10 µl 
 Pct Recovery = 107%  Analysis Date = 10/23/15 
 SpikeMix = Abs 040315: 10 µl & ChemService 3818700: 10 µl 
 Pct Recovery = 98%  Analysis Date = 08/14/15 
 SpikeMix = Abs 040315: 10 µl & ERA 0601-15-05: 10 µl 
 Pct Recovery = 98%  Analysis Date = 05/05/15 
 SpikeMix = Supelco LC13544: 10 µl & Abs 040315: 10 µl 
 Pct Recovery = 93%  Analysis Date = 08/10/16 
 Pct Recovery = 101%  Analysis Date = 08/06/16 
 Pct Recovery = 101%  Analysis Date = 08/06/16 
 Pct Recovery = 101%  Analysis Date = 08/02/16 
 Pct Recovery = 101%  Analysis Date = 08/02/16 
 Pct Recovery = 101%  Analysis Date = 07/29/16 
 Pct Recovery = 101%  Analysis Date = 07/29/16 
 Pct Recovery = 101%  Analysis Date = 07/25/16 
 Pct Recovery = 101%  Analysis Date = 07/25/16 
 Pct Recovery = 101%  Analysis Date = 07/21/16 
 Pct Recovery = 101%  Analysis Date = 07/21/16 
 Pct Recovery = 101%  Analysis Date = 07/17/16 
 Pct Recovery = 101%  Analysis Date = 07/17/16 
 Pct Recovery = 101%  Analysis Date = 07/13/16 
 Pct Recovery = 101%  Analysis Date = 07/13/16 
 Pct Recovery = 101%  Analysis Date = 07/08/16 
 Pct Recovery = 101%  Analysis Date = 07/08/16 
 Pct Recovery = 101%  Analysis Date = 07/04/16 
 Pct Recovery = 101%  Analysis Date = 07/04/16 
 Pct Recovery = 101%  Analysis Date = 06/30/16 
 Pct Recovery = 101%  Analysis Date = 06/30/16 
 Pct Recovery = 101%  Analysis Date = 06/26/16 
 Pct Recovery = 101%  Analysis Date = 06/26/16 
 Pct Recovery = 101%  Analysis Date = 06/22/16 
 Pct Recovery = 101%  Analysis Date = 06/22/16 
 Pct Recovery = 101%  Analysis Date = 06/18/16 
 Pct Recovery = 101%  Analysis Date = 06/18/16 
 Pct Recovery = 101%  Analysis Date = 06/14/16 
 Pct Recovery = 101%  Analysis Date = 06/14/16 
 Pct Recovery = 101%  Analysis Date = 06/09/16 
 Pct Recovery = 101%  Analysis Date = 06/09/16 
 Pct Recovery = 101%  Analysis Date = 06/05/16 
 Pct Recovery = 101%  Analysis Date = 06/05/16 
 Pct Recovery = 101%  Analysis Date = 06/01/16 
 Pct Recovery = 101%  Analysis Date = 06/01/16 
 Pct Recovery = 101%  Analysis Date = 05/28/16 
 Pct Recovery = 101%  Analysis Date = 05/28/16 
 Pct Recovery = 101%  Analysis Date = 05/24/16 
 Pct Recovery = 101%  Analysis Date = 05/24/16 
 Pct Recovery = 101%  Analysis Date = 05/20/16 
 Pct Recovery = 101%  Analysis Date = 05/20/16 
 Pct Recovery = 101%  Analysis Date = 05/16/16 
 Pct Recovery = 101%  Analysis Date = 05/16/16 
 Pct Recovery = 101%  Analysis Date = 05/12/16 
 Pct Recovery = 101%  Analysis Date = 05/12/16 
 Pct Recovery = 101%  Analysis Date = 05/07/16 
 Pct Recovery = 101%  Analysis Date = 05/07/16 
 Pct Recovery = 101%  Analysis Date = 05/03/16 
 Pct Recovery = 101%  Analysis Date = 05/03/16 
 Pct Recovery = 101%  Analysis Date = 04/29/16 
 Pct Recovery = 101%  Analysis Date = 04/29/16 
 Pct Recovery = 101%  Analysis Date = 04/25/16 
 Pct Recovery = 101%  Analysis Date = 04/25/16 
 Pct Recovery = 101%  Analysis Date = 04/21/16 
 Pct Recovery = 101%  Analysis Date = 04/21/16 
 Pct Recovery = 101%  Analysis Date = 04/17/16 
 Pct Recovery = 101%  Analysis Date = 04/17/16 
 Pct Recovery = 101%  Analysis Date = 04/13/16 
 Pct Recovery = 101%  Analysis Date = 04/13/16 
 Pct Recovery = 101%  Analysis Date = 04/08/16 
 Pct Recovery = 102%  Analysis Date = 04/08/16 
 Pct Recovery = 102%  Analysis Date = 04/04/16 
 Pct Recovery = 102%  Analysis Date = 04/04/16 
 Pct Recovery = 102%  Analysis Date = 03/31/16 
 Pct Recovery = 102%  Analysis Date = 03/31/16 
 Pct Recovery = 102%  Analysis Date = 03/27/16 
 Pct Recovery = 102%  Analysis Date = 03/27/16 
 Pct Recovery = 102%  Analysis Date = 03/23/16 
 Pct Recovery = 102%  Analysis Date = 03/23/16 
 Pct Recovery = 102%  Analysis Date = 03/19/16 
 Pct Recovery = 102%  Analysis Date = 03/19/16 
 Pct Recovery = 102%  Analysis Date = 03/15/16 
 Pct Recovery = 102%  Analysis Date = 03/15/16 
 Pct Recovery = 102%  Analysis Date = 03/11/16 
 Pct Recovery = 102%  Analysis Date = 03/11/16 
 Pct Recovery = 102%  Analysis Date = 03/06/16 
 Pct Recovery = 102%  Analysis Date = 03/06/16 
 Pct Recovery = 102%  Analysis Date = 03/02/16 
 Pct Recovery = 102%  Analysis Date = 03/02/16 
 Pct Recovery = 102%  Analysis Date = 02/27/16 
 Pct Recovery = 102%  Analysis Date = 02/27/16 
 Pct Recovery = 102%  Analysis Date = 02/23/16 
 Pct Recovery = 102%  Analysis Date = 02/23/16 
 Pct Recovery = 102%  Analysis Date = 02/19/16 
 Pct Recovery = 102%  Analysis Date = 02/19/16 
 Pct Recovery = 102%  Analysis Date = 02/15/16 
 Pct Recovery = 102%  Analysis Date = 02/15/16 
 Pct Recovery = 102%  Analysis Date = 02/11/16 
 Pct Recovery = 102%  Analysis Date = 02/11/16 
 Pct Recovery = 102%  Analysis Date = 02/06/16 
 Pct Recovery = 102%  Analysis Date = 02/06/16 
 Pct Recovery = 102%  Analysis Date = 02/02/16 
 Pct Recovery = 102%  Analysis Date = 02/02/16 
 Pct Recovery = 102%  Analysis Date = 01/29/16 
 Pct Recovery = 102%  Analysis Date = 01/29/16 
 Pct Recovery = 102%  Analysis Date = 01/25/16 
 Pct Recovery = 102%  Analysis Date = 01/25/16 
 Pct Recovery = 102%  Analysis Date = 01/21/16 
 Pct Recovery = 102%  Analysis Date = 01/21/16 
 Pct Recovery = 102%  Analysis Date = 01/17/16 
 Pct Recovery = 102%  Analysis Date = 01/17/16 
 Pct Recovery = 102%  Analysis Date = 01/13/16 
 Pct Recovery = 102%  Analysis Date = 01/13/16 
 Pct Recovery = 102%  Analysis Date = 01/08/16 
 Pct Recovery = 102%  Analysis Date = 01/08/16 
 Pct Recovery = 102%  Analysis Date = 01/04/16 
 Pct Recovery = 102%  Analysis Date = 01/04/16 
 Pct Recovery = 102%  Analysis Date = 12/31/15 
 Pct Recovery = 102%  Analysis Date = 12/31/15 
 Pct Recovery = 102%  Analysis Date = 12/27/15 
 Pct Recovery = 102%  Analysis Date = 12/27/15 
 Pct Recovery = 102%  Analysis Date = 12/23/15 
 Pct Recovery = 102%  Analysis Date = 12/23/15 
 Pct Recovery = 102%  Analysis Date = 12/19/15 
 Pct Recovery = 102%  Analysis Date = 12/19/15 
 Pct Recovery = 102%  Analysis Date = 12/15/15 
 Pct Recovery = 102%  Analysis Date = 12/15/15 
 Pct Recovery = 102%  Analysis Date = 12/11/15 
 Pct Recovery = 101%  Analysis Date = 12/11/15 
 Pct Recovery = 101%  Analysis Date = 12/06/15 
 Pct Recovery = 101%  Analysis Date = 12/06/15 
 Pct Recovery = 101%  Analysis Date = 12/02/15 
 Pct Recovery = 101%  Analysis Date = 12/02/15 
 Pct Recovery = 101%  Analysis Date = 11/28/15 
 Pct Recovery = 101%  Analysis Date = 11/28/15 
 Pct Recovery = 101%  Analysis Date = 11/24/15 
 Pct Recovery = 101%  Analysis Date = 11/24/15 
 Pct Recovery = 101%  Analysis Date = 11/20/15 
 Pct Recovery = 101%  Analysis Date = 11/20/15 
 Pct Recovery = 101%  Analysis Date = 11/16/15 
 Pct Recovery = 101%  Analysis Date = 11/16/15 
 Pct Recovery = 101%  Analysis Date = 11/12/15 
 Pct Recovery = 101%  Analysis Date = 11/12/15 
 Pct Recovery = 101%  Analysis Date = 11/07/15 
 Pct Recovery = 101%  Analysis Date = 11/07/15 
 Pct Recovery = 101%  Analysis Date = 11/03/15 
 Pct Recovery = 101%  Analysis Date = 11/03/15 
 Pct Recovery = 101%  Analysis Date = 10/30/15 
 Pct Recovery = 101%  Analysis Date = 10/30/15 
 Pct Recovery = 101%  Analysis Date = 10/26/15 
 Pct Recovery = 101%  Analysis Date = 10/26/15 
 Pct Recovery = 101%  Analysis Date = 10/22/15 
 Pct Recovery = 101%  Analysis Date = 10/22/15 
 Pct Recovery = 101%  Analysis Date = 10/18/15 
 Pct Recovery = 101%  Analysis Date = 10/18/15 
 Pct Recovery = 101%  Analysis Date = 10/14/15 
 Pct Recovery = 101%  Analysis Date = 10/14/15 
 Pct Recovery = 101%  Analysis Date = 10/10/15 
 Pct Recovery = 101%  Analysis Date = 10/10/15 
 Pct Recovery = 101%  Analysis Date = 10/05/15 
 Pct Recovery = 101%  Analysis Date = 10/05/15 
 Pct Recovery = 101%  Analysis Date = 10/01/15 
 Pct Recovery = 101%  Analysis Date = 10/01/15 
 Pct Recovery = 101%  Analysis Date = 09/27/15 
 Pct Recovery = 101%  Analysis Date = 09/27/15 
 Pct Recovery = 101%  Analysis Date = 09/23/15 
 Pct Recovery = 100%  Analysis Date = 09/23/15 
 Pct Recovery = 100%  Analysis Date = 09/19/15 
 Pct Recovery = 100%  Analysis Date = 09/19/15 
 Pct Recovery = 100%  Analysis Date = 09/15/15 
 Pct Recovery = 100%  Analysis Date = 09/15/15 
 Pct Recovery = 100%  Analysis Date = 09/11/15 
 Pct Recovery = 100%  Analysis Date = 09/11/15 
 Pct Recovery = 100%  Analysis Date = 09/06/15 
 Pct Recovery = 100%  Analysis Date = 09/06/15 
 Pct Recovery = 100%  Analysis Date = 09/02/15 
 Pct Recovery = 100%  Analysis Date = 09/02/15 
 Pct Recovery = 100%  Analysis Date = 08/29/15 
 Pct Recovery = 100%  Analysis Date = 08/29/15 
 Pct Recovery = 100%  Analysis Date = 08/25/15 
 Pct Recovery = 100%  Analysis Date = 08/25/15 
 Pct Recovery = 100%  Analysis Date = 08/21/15 
 Pct Recovery = 100%  Analysis Date = 08/21/15 
 Pct Recovery = 100%  Analysis Date = 08/17/15 
 Pct Recovery = 99%  Analysis Date = 08/17/15 
 Pct Recovery = 99%  Analysis Date = 08/13/15 
 Pct Recovery = 99%  Analysis Date = 08/13/15 
 Pct Recovery = 99%  Analysis Date = 08/08/15 
 Pct Recovery = 99%  Analysis Date = 08/08/15 
 Pct Recovery = 99%  Analysis Date = 08/04/15 
 Pct Recovery = 99%  Analysis Date = 08/04/15 
 Pct Recovery = 99%  Analysis Date = 07/31/15 
 Pct Recovery = 99%  Analysis Date = 07/31/15 
 Pct Recovery = 99%  Analysis Date = 07/27/15 
 Pct Recovery = 99%  Analysis Date = 07/27/15 
 Pct Recovery = 99%  Analysis Date = 07/23/15 
 Pct Recovery = 99%  Analysis Date = 07/23/15 
 Pct Recovery = 99%  Analysis Date = 07/19/15 
 Pct Recovery = 99%  Analysis Date = 07/19/15 
 Pct Recovery = 99%  Analysis Date = 07/15/15 
 Pct Recovery = 99%  Analysis Date = 07/15/15 
 Pct Recovery = 99%  Analysis Date = 07/11/15 
 Pct Recovery = 99%  Analysis Date = 07/11/15 
 Pct Recovery = 99%  Analysis Date = 07/06/15 
 Pct Recovery = 98%  Analysis Date = 07/06/15 
 Pct Recovery = 98%  Analysis Date = 07/02/15 
 Pct Recovery = 98%  Analysis Date = 07/02/15 
 Pct Recovery = 98%  Analysis Date = 06/28/15 
 Pct Recovery = 98%  Analysis Date = 06/28/15 
 Pct Recovery = 98%  Analysis Date = 06/24/15 
 Pct Recovery = 98%  Analysis Date = 06/24/15 
 Pct Recovery = 98%  Analysis Date = 06/20/15 
 Pct Recovery = 98%  Analysis Date = 06/20/15 
 Pct Recovery = 98%  Analysis Date = 06/16/15 
 Pct Recovery = 98%  Analysis Date = 06/16/15 
 Pct Recovery = 98%  Analysis Date = 06/12/15 
 Pct Recovery = 98%  Analysis Date = 06/12/15 
 Pct Recovery = 98%  Analysis Date = 06/07/15 
 Pct Recovery = 98%  Analysis Date = 06/07/15 
 Pct Recovery = 98%  Analysis Date = 06/03/15 
 Pct Recovery = 98%  Analysis Date = 06/03/15 
 Pct Recovery = 98%  Analysis Date = 05/30/15 
 Pct Recovery = 98%  Analysis Date = 05/30/15 
 Pct Recovery = 98%  Analysis Date = 05/26/15 
 Pct Recovery = 97%  Analysis Date = 05/26/15 
 Pct Recovery = 97%  Analysis Date = 05/22/15 
 Pct Recovery = 97%  Analysis Date = 05/22/15 
 Pct Recovery = 97%  Analysis Date = 05/18/15 
 Pct Recovery = 97%  Analysis Date = 05/18/15 
 Pct Recovery = 97%  Analysis Date = 05/14/15 
 Pct Recovery = 97%  Analysis Date = 05/14/15 
 Pct Recovery = 97%  Analysis Date = 05/10/15 
 Pct Recovery = 97%  Analysis Date = 05/10/15 
 Pct Recovery = 97%  Analysis Date = 05/05/15 
 Pct Recovery = 97%  Analysis Date = 05/05/15 
 Pct Recovery = 97%  Analysis Date = 05/01/15 
 Pct Recovery = 97%  Analysis Date = 05/01/15 
 Pct Recovery = 97%  Analysis Date = 04/27/15 
 Pct Recovery = 97%  Analysis Date = 04/27/15 
 Pct Recovery = 97%  Analysis Date = 04/23/15 
 Pct Recovery = 97%  Analysis Date = 04/23/15 
 Pct Recovery = 97%  Analysis Date = 04/19/15 
 Pct Recovery = 97%  Analysis Date = 04/19/15 
 Pct Recovery = 97%  Analysis Date = 04/15/15 
 Pct Recovery = 96%  Analysis Date = 04/15/15 
 Pct Recovery = 96%  Analysis Date = 04/11/15 
 Pct Recovery = 96%  Analysis Date = 04/11/15 
 Pct Recovery = 96%  Analysis Date = 04/06/15 
 Pct Recovery = 96%  Analysis Date = 04/06/15 
 Pct Recovery = 96%  Analysis Date = 04/02/15 
 Pct Recovery = 96%  Analysis Date = 04/02/15 
 Pct Recovery = 96%  Analysis Date = 03/29/15 
 Pct Recovery = 96%  Analysis Date = 03/29/15 
 Pct Recovery = 96%  Analysis Date = 03/25/15 
 Pct Recovery = 96%  Analysis Date = 03/25/15 
 Pct Recovery = 96%  Analysis Date = 03/21/15 
 Pct Recovery = 96%  Analysis Date = 03/21/15 
 Pct Recovery = 96%  Analysis Date = 03/17/15 
 Pct Recovery = 96%  Analysis Date = 03/17/15 
 Pct Recovery = 96%  Analysis Date = 03/13/15 
 Pct Recovery = 96%  Analysis Date = 03/13/15 
 Pct Recovery = 96%  Analysis Date = 03/08/15 
 Pct Recovery = 96%  Analysis Date = 03/08/15 
 Pct Recovery = 96%  Analysis Date = 03/04/15 
 Pct Recovery = 95%  Analysis Date = 03/04/15 
 Pct Recovery = 95%  Analysis Date = 02/28/15 
 Pct Recovery = 95%  Analysis Date = 02/28/15 
 Pct Recovery = 95%  Analysis Date = 02/24/15 
 Pct Recovery = 95%  Analysis Date = 02/24/15 
 Pct Recovery = 95%  Analysis Date = 02/20/15 
 Pct Recovery = 95%  Analysis Date = 02/20/15 
 Pct Recovery = 95%  Analysis Date = 02/16/15 
 Pct Recovery = 95%  Analysis Date = 02/16/15 
 Pct Recovery = 95%  Analysis Date = 02/12/15 
 Pct Recovery = 95%  Analysis Date = 02/12/15 
 Pct Recovery = 95%  Analysis Date = 02/08/15 
 Pct Recovery = 95%  Analysis Date = 02/08/15 
 Pct Recovery = 95%  Analysis Date = 02/03/15 
 Pct Recovery = 95%  Analysis Date = 02/03/15 
 Pct Recovery = 95%  Analysis Date = 01/30/15 
 Pct Recovery = 94%  Analysis Date = 01/30/15 
 Pct Recovery = 94%  Analysis Date = 01/26/15 
 Pct Recovery = 94%  Analysis Date = 01/26/15 
 Pct Recovery = 94%  Analysis Date = 01/22/15 
 Pct Recovery = 94%  Analysis Date = 01/22/15 
 Pct Recovery = 94%  Analysis Date = 01/18/15 
 Pct Recovery = 94%  Analysis Date = 01/18/15 
 Pct Recovery = 94%  Analysis Date = 01/14/15 
 Pct Recovery = 94%  Analysis Date = 01/14/15 
 Pct Recovery = 94%  Analysis Date = 01/10/15 
 Pct Recovery = 94%  Analysis Date = 01/10/15 
 Pct Recovery = 94%  Analysis Date = 01/05/15 
 Pct Recovery = 94%  Analysis Date = 01/05/15 
 Pct Recovery = 94%  Analysis Date = 01/01/15 
 Pct Recovery = 94%  Analysis Date = 01/01/15 
 Pct Recovery = 94%  Analysis Date = 12/28/14 
 Pct Recovery = 93%  Analysis Date = 12/28/14 
 Pct Recovery = 93%  Analysis Date = 12/24/14 
 Pct Recovery = 93%  Analysis Date = 12/24/14 
 Pct Recovery = 93%  Analysis Date = 12/20/14 
 Pct Recovery = 93%  Analysis Date = 12/20/14 
 Pct Recovery = 93%  Analysis Date = 12/16/14 
 Pct Recovery = 93%  Analysis Date = 12/16/14 
 Pct Recovery = 93%  Analysis Date = 12/12/14 
 Pct Recovery = 93%  Analysis Date = 12/12/14 
 Pct Recovery = 93%  Analysis Date = 12/08/14 
 Pct Recovery = 93%  Analysis Date = 12/08/14 
 Pct Recovery = 93%  Analysis Date = 12/03/14 
 Pct Recovery = 93%  Analysis Date = 12/03/14 
 Pct Recovery = 93%  Analysis Date = 11/29/14 
 Pct Recovery = 93%  Analysis Date = 11/29/14 
 Pct Recovery = 93%  Analysis Date = 11/25/14 
 Pct Recovery = 92%  Analysis Date = 11/25/14 
 Pct Recovery = 92%  Analysis Date = 11/21/14 
 Pct Recovery = 92%  Analysis Date = 11/21/14 
 Pct Recovery = 92%  Analysis Date = 11/17/14 
 Pct Recovery = 92%  Analysis Date = 11/17/14 
 Pct Recovery = 92%  Analysis Date = 11/13/14 
 Pct Recovery = 92%  Analysis Date = 11/13/14 
 Pct Recovery = 92%  Analysis Date = 11/09/14 
 Pct Recovery = 92%  Analysis Date = 11/09/14 
 Pct Recovery = 92%  Analysis Date = 11/04/14 
 Pct Recovery = 92%  Analysis Date = 11/04/14 
 Pct Recovery = 92%  Analysis Date = 10/31/14 
 Pct Recovery = 92%  Analysis Date = 10/31/14 
 Pct Recovery = 92%  Analysis Date = 10/27/14 
 Pct Recovery = 92%  Analysis Date = 10/27/14 
 Pct Recovery = 92%  Analysis Date = 10/23/14 
 Pct Recovery = 92%  Analysis Date = 10/23/14 
 Pct Recovery = 92%  Analysis Date = 10/19/14 
 Pct Recovery = 92%  Analysis Date = 10/19/14 
 Pct Recovery = 92%  Analysis Date = 10/15/14 
 Pct Recovery = 92%  Analysis Date = 10/15/14 
 Pct Recovery = 92%  Analysis Date = 10/11/14 
 Pct Recovery = 92%  Analysis Date = 10/11/14 
 Pct Recovery = 92%  Analysis Date = 10/06/14 
 Pct Recovery = 91%  Analysis Date = 10/06/14 
 Pct Recovery = 91%  Analysis Date = 10/02/14 
 Pct Recovery = 91%  Analysis Date = 10/02/14 
 Pct Recovery = 91%  Analysis Date = 09/28/14 
 Pct Recovery = 91%  Analysis Date = 09/28/14 
 Pct Recovery = 91%  Analysis Date = 09/24/14 
 Pct Recovery = 91%  Analysis Date = 09/24/14 
 Pct Recovery = 91%  Analysis Date = 09/20/14 
 Pct Recovery = 91%  Analysis Date = 09/20/14 
 Pct Recovery = 91%  Analysis Date = 09/16/14 
 Pct Recovery = 91%  Analysis Date = 09/16/14 
 Pct Recovery = 91%  Analysis Date = 09/12/14 
 Pct Recovery = 91%  Analysis Date = 09/12/14 
 Pct Recovery = 91%  Analysis Date = 09/08/14 
 Pct Recovery = 91%  Analysis Date = 09/08/14 
 Pct Recovery = 91%  Analysis Date = 09/03/14 
 Pct Recovery = 91%  Analysis Date = 09/03/14 
 Pct Recovery = 91%  Analysis Date = 08/30/14 
 Pct Recovery = 91%  Analysis Date = 08/30/14 
 Pct Recovery = 91%  Analysis Date = 08/26/14 
 Pct Recovery = 91%  Analysis Date = 08/26/14 
 Pct Recovery = 91%  Analysis Date = 08/22/14 
 Pct Recovery = 91%  Analysis Date = 08/22/14 
 Pct Recovery = 91%  Analysis Date = 08/18/14 
 Pct Recovery = 91%  Analysis Date = 08/18/14 
 Pct Recovery = 91%  Analysis Date = 08/14/14 
 Pct Recovery = 90%  Analysis Date = 08/14/14 
 Pct Recovery = 90%  Analysis Date = 08/10/14 
 Pct Recovery = 90%  Analysis Date = 08/10/14 
 Pct Recovery = 90%  Analysis Date = 08/05/14 
 Pct Recovery = 90%  Analysis Date = 08/05/14 
 Pct Recovery = 90%  Analysis Date = 08/01/14 
 Pct Recovery = 90%  Analysis Date = 08/01/14 
 Pct Recovery = 90%  Analysis Date = 07/28/14 
 Pct Recovery = 90%  Analysis Date = 07/28/14 
 Pct Recovery = 90%  Analysis Date = 07/24/14 
 Pct Recovery = 90%  Analysis Date = 07/24/14 
 Pct Recovery = 90%  Analysis Date = 07/20/14 
 Pct Recovery = 90%  Analysis Date = 07/20/14 
 Pct Recovery = 90%  Analysis Date = 07/16/14 
 Pct Recovery = 90%  Analysis Date = 07/16/14 
 Pct Recovery = 90%  Analysis Date = 07/12/14 
 Pct Recovery = 90%  Analysis Date = 07/12/14 
 Pct Recovery = 90%  Analysis Date = 07/08/14 
 Pct Recovery = 90%  Analysis Date = 07/08/14 
 Pct Recovery = 90%  Analysis Date = 07/03/14 
 Pct Recovery = 90%  Analysis Date = 07/03/14 
 Pct Recovery = 90%  Analysis Date = 06/29/14 
 Pct Recovery = 90%  Analysis Date = 06/29/14 
 Pct Recovery = 90%  Analysis Date = 06/25/14 
 Pct Recovery = 89%  Analysis Date = 06/25/14 
 Pct Recovery = 89%  Analysis Date = 06/21/14 
 Pct Recovery = 89%  Analysis Date = 06/21/14 
 Pct Recovery = 89%  Analysis Date = 06/17/14 
 Pct Recovery = 89%  Analysis Date = 06/17/14 
 Pct Recovery = 89%  Analysis Date = 06/13/14 
 Pct Recovery = 89%  Analysis Date = 06/13/14 
 Pct Recovery = 89%  Analysis Date = 06/09/14 
 Pct Recovery = 89%  Analysis Date = 06/09/14 
 Pct Recovery = 89%  Analysis Date = 06/04/14 
 Pct Recovery = 89%  Analysis Date = 06/04/14 
 Pct Recovery = 89%  Analysis Date = 05/31/14 
 Pct Recovery = 89%  Analysis Date = 05/31/14 
 Pct Recovery = 89%  Analysis Date = 05/27/14 
 Pct Recovery = 89%  Analysis Date = 05/27/14 
 Pct Recovery = 89%  Analysis Date = 05/23/14 
 Pct Recovery = 89%  Analysis Date = 05/23/14 
 Pct Recovery = 89%  Analysis Date = 05/19/14 
 Pct Recovery = 89%  Analysis Date = 05/19/14 
 Pct Recovery = 89%  Analysis Date = 05/15/14 
 Pct Recovery = 89%  Analysis Date = 05/15/14 
 Pct Recovery = 89%  Analysis Date = 05/11/14 
 Pct Recovery = 89%  Analysis Date = 05/11/14 
 Pct Recovery = 89%  Analysis Date = 05/07/14 
 Pct Recovery = 89%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
1,2,3-TRICHLOROPROPANE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 36 97% 8% 96% 7%
Total 36 97% 8% 96% 7%

Sample Statistics
1,2,3-TRICHLOROPROPANE

Characteristic N % % Basis
Plotted 36 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 36 .  
False Negatives 0 0% 0 out of 36
Not Spiked 19 .  
False Positives 0 0% 0 out of 19

BQS OBSP Determination:
1,2-DIBROMO-3-CHLOROPROPANE
METHOD: 4437 , TESTIDCODE: 82625GM016
Open Data Set

 Analysis Date = 03/19/15 
 SpikeMix = Supelco LC06437: 20 µl & NSI 031814: 20 µl 
 Pct Recovery = 101%  Analysis Date = 01/10/15 
 SpikeMix = Abs 032014: 20 µl & ERA 0321-14-05A: 20 µl 
 Pct Recovery = 100%  Analysis Date = 08/20/14 
 SpikeMix = Supelco LC06437: 20 µl & Abs 032014: 20 µl 
 Pct Recovery = 99%  Analysis Date = 07/23/14 
 SpikeMix = Accu 214031128: 20 µl & Abs 032014: 20 µl 
 Pct Recovery = 104%  Analysis Date = 07/03/14 
 SpikeMix = Abs 032014: 20 µl & ChemService 2615700: 20 µl 
 Pct Recovery = 100%  Analysis Date = 06/06/14 
 SpikeMix = NSI 031814: 20 µl & ChemService 2615700: 20 µl 
 Pct Recovery = 106%  Analysis Date = 05/07/14 
 SpikeMix = NSI 031814: 20 µl & Accu 214031128: 20 µl 
 Pct Recovery = 102%  Analysis Date = 01/22/16 
 SpikeMix = NSI 050515HVOC: 25 µl & ERA 0601-15-05: 25 µl 
 Pct Recovery = 92%  Analysis Date = 10/09/15 
 SpikeMix = ERA 0601-15-05: 25 µl & Accu 215041338: 25 µl 
 Pct Recovery = 104%  Analysis Date = 06/26/15 
 SpikeMix = ChemService 3818700: 25 µl & Accu 215041338: 25 µl 
 Pct Recovery = 101%  Analysis Date = 06/25/15 
 SpikeMix = ChemService 3818700: 25 µl & NSI 050515HVOC: 25 µl 
 Pct Recovery = 96%  Analysis Date = 08/12/16 
 SpikeMix = Accu 216041354: 15 µl & Abs 060916HVOC: 15 µl 
 Pct Recovery = 86%  Analysis Date = 09/24/15 
 SpikeMix = Abs 040315: 15 µl & ERA 0601-15-05: 15 µl 
 Pct Recovery = 99%  Analysis Date = 08/24/15 
 SpikeMix = ERA 0601-15-05: 15 µl & Supelco LC13544: 15 µl 
 Pct Recovery = 109%  Analysis Date = 04/28/16 
 SpikeMix = ChemService 3818700: 15 µl & Supelco LC13544: 15 µl 
 Pct Recovery = 99%  Analysis Date = 06/16/15 
 SpikeMix = ChemService 3818700: 15 µl & NSI 050515HVOC: 15 µl 
 Pct Recovery = 92%  Analysis Date = 05/14/15 
 SpikeMix = ChemService 3818700: 15 µl & Supelco LC13544: 15 µl 
 Pct Recovery = 100%  Analysis Date = 04/25/15 
 SpikeMix = Abs 032014: 10 µl & ERA 0321-14-05A: 10 µl 
 Pct Recovery = 99%  Analysis Date = 12/13/14 
 SpikeMix = Accu 214031128: 10 µl & NSI 031814: 10 µl 
 Pct Recovery = 106%  Analysis Date = 09/11/14 
 SpikeMix = Accu 214031128: 10 µl & Abs 032014: 10 µl 
 Pct Recovery = 107%  Analysis Date = 07/30/14 
 SpikeMix = NSI 031814: 10 µl & ChemService 2615700: 10 µl 
 Pct Recovery = 101%  Analysis Date = 06/17/14 
 SpikeMix = Supelco LC06437: 10 µl & Abs 032014: 10 µl 
 Pct Recovery = 109%  Analysis Date = 02/12/16 
 SpikeMix = ERA 0601-15-05: 10 µl & Accu 215041338: 10 µl 
 Pct Recovery = 104%  Analysis Date = 12/05/15 
 SpikeMix = NSI 050515HVOC: 10 µl & ERA 0601-15-05: 10 µl 
 Pct Recovery = 107%  Analysis Date = 11/14/15 
 SpikeMix = ERA 0601-15-05: 10 µl 
 Pct Recovery = 100%  Analysis Date = 08/14/15 
 SpikeMix = Abs 040315: 10 µl & ERA 0601-15-05: 10 µl 
 Pct Recovery = 89%  Analysis Date = 04/09/16 
 SpikeMix = Abs 040315: 10 µl & ChemService 3818700: 10 µl 
 Pct Recovery = 90%  Analysis Date = 12/10/15 
 SpikeMix = ChemService 3818700: 10 µl & Supelco LC13544: 10 µl 
 Pct Recovery = 105%  Analysis Date = 10/23/15 
 SpikeMix = Abs 040315: 10 µl & ChemService 3818700: 10 µl 
 Pct Recovery = 105%  Analysis Date = 05/20/15 
 SpikeMix = ChemService 3818700: 10 µl & Accu 215041338: 10 µl 
 Pct Recovery = 115%  Analysis Date = 08/11/16 
 Pct Recovery = 89%  Analysis Date = 08/07/16 
 Pct Recovery = 89%  Analysis Date = 08/07/16 
 Pct Recovery = 89%  Analysis Date = 08/03/16 
 Pct Recovery = 89%  Analysis Date = 08/03/16 
 Pct Recovery = 89%  Analysis Date = 07/30/16 
 Pct Recovery = 89%  Analysis Date = 07/30/16 
 Pct Recovery = 89%  Analysis Date = 07/26/16 
 Pct Recovery = 89%  Analysis Date = 07/26/16 
 Pct Recovery = 89%  Analysis Date = 07/22/16 
 Pct Recovery = 90%  Analysis Date = 07/22/16 
 Pct Recovery = 90%  Analysis Date = 07/18/16 
 Pct Recovery = 90%  Analysis Date = 07/18/16 
 Pct Recovery = 90%  Analysis Date = 07/14/16 
 Pct Recovery = 90%  Analysis Date = 07/14/16 
 Pct Recovery = 90%  Analysis Date = 07/09/16 
 Pct Recovery = 90%  Analysis Date = 07/09/16 
 Pct Recovery = 90%  Analysis Date = 07/05/16 
 Pct Recovery = 91%  Analysis Date = 07/05/16 
 Pct Recovery = 91%  Analysis Date = 07/01/16 
 Pct Recovery = 91%  Analysis Date = 07/01/16 
 Pct Recovery = 91%  Analysis Date = 06/27/16 
 Pct Recovery = 91%  Analysis Date = 06/27/16 
 Pct Recovery = 91%  Analysis Date = 06/23/16 
 Pct Recovery = 91%  Analysis Date = 06/23/16 
 Pct Recovery = 91%  Analysis Date = 06/19/16 
 Pct Recovery = 91%  Analysis Date = 06/19/16 
 Pct Recovery = 91%  Analysis Date = 06/15/16 
 Pct Recovery = 92%  Analysis Date = 06/15/16 
 Pct Recovery = 92%  Analysis Date = 06/10/16 
 Pct Recovery = 92%  Analysis Date = 06/10/16 
 Pct Recovery = 92%  Analysis Date = 06/06/16 
 Pct Recovery = 92%  Analysis Date = 06/06/16 
 Pct Recovery = 92%  Analysis Date = 06/02/16 
 Pct Recovery = 92%  Analysis Date = 06/02/16 
 Pct Recovery = 92%  Analysis Date = 05/29/16 
 Pct Recovery = 92%  Analysis Date = 05/29/16 
 Pct Recovery = 92%  Analysis Date = 05/25/16 
 Pct Recovery = 93%  Analysis Date = 05/25/16 
 Pct Recovery = 93%  Analysis Date = 05/21/16 
 Pct Recovery = 93%  Analysis Date = 05/21/16 
 Pct Recovery = 93%  Analysis Date = 05/17/16 
 Pct Recovery = 93%  Analysis Date = 05/17/16 
 Pct Recovery = 93%  Analysis Date = 05/12/16 
 Pct Recovery = 93%  Analysis Date = 05/12/16 
 Pct Recovery = 93%  Analysis Date = 05/08/16 
 Pct Recovery = 94%  Analysis Date = 05/08/16 
 Pct Recovery = 94%  Analysis Date = 05/04/16 
 Pct Recovery = 94%  Analysis Date = 05/04/16 
 Pct Recovery = 94%  Analysis Date = 04/30/16 
 Pct Recovery = 94%  Analysis Date = 04/30/16 
 Pct Recovery = 94%  Analysis Date = 04/26/16 
 Pct Recovery = 94%  Analysis Date = 04/26/16 
 Pct Recovery = 94%  Analysis Date = 04/22/16 
 Pct Recovery = 94%  Analysis Date = 04/22/16 
 Pct Recovery = 94%  Analysis Date = 04/18/16 
 Pct Recovery = 95%  Analysis Date = 04/18/16 
 Pct Recovery = 95%  Analysis Date = 04/13/16 
 Pct Recovery = 95%  Analysis Date = 04/13/16 
 Pct Recovery = 95%  Analysis Date = 04/09/16 
 Pct Recovery = 95%  Analysis Date = 04/09/16 
 Pct Recovery = 95%  Analysis Date = 04/05/16 
 Pct Recovery = 95%  Analysis Date = 04/05/16 
 Pct Recovery = 95%  Analysis Date = 04/01/16 
 Pct Recovery = 95%  Analysis Date = 04/01/16 
 Pct Recovery = 95%  Analysis Date = 03/28/16 
 Pct Recovery = 96%  Analysis Date = 03/28/16 
 Pct Recovery = 96%  Analysis Date = 03/24/16 
 Pct Recovery = 96%  Analysis Date = 03/24/16 
 Pct Recovery = 96%  Analysis Date = 03/20/16 
 Pct Recovery = 96%  Analysis Date = 03/20/16 
 Pct Recovery = 96%  Analysis Date = 03/15/16 
 Pct Recovery = 96%  Analysis Date = 03/15/16 
 Pct Recovery = 96%  Analysis Date = 03/11/16 
 Pct Recovery = 97%  Analysis Date = 03/11/16 
 Pct Recovery = 97%  Analysis Date = 03/07/16 
 Pct Recovery = 97%  Analysis Date = 03/07/16 
 Pct Recovery = 97%  Analysis Date = 03/03/16 
 Pct Recovery = 97%  Analysis Date = 03/03/16 
 Pct Recovery = 97%  Analysis Date = 02/28/16 
 Pct Recovery = 97%  Analysis Date = 02/28/16 
 Pct Recovery = 97%  Analysis Date = 02/24/16 
 Pct Recovery = 97%  Analysis Date = 02/24/16 
 Pct Recovery = 97%  Analysis Date = 02/20/16 
 Pct Recovery = 98%  Analysis Date = 02/20/16 
 Pct Recovery = 98%  Analysis Date = 02/15/16 
 Pct Recovery = 98%  Analysis Date = 02/15/16 
 Pct Recovery = 98%  Analysis Date = 02/11/16 
 Pct Recovery = 98%  Analysis Date = 02/11/16 
 Pct Recovery = 98%  Analysis Date = 02/07/16 
 Pct Recovery = 98%  Analysis Date = 02/07/16 
 Pct Recovery = 98%  Analysis Date = 02/03/16 
 Pct Recovery = 98%  Analysis Date = 02/03/16 
 Pct Recovery = 98%  Analysis Date = 01/30/16 
 Pct Recovery = 98%  Analysis Date = 01/30/16 
 Pct Recovery = 98%  Analysis Date = 01/26/16 
 Pct Recovery = 99%  Analysis Date = 01/26/16 
 Pct Recovery = 99%  Analysis Date = 01/22/16 
 Pct Recovery = 99%  Analysis Date = 01/22/16 
 Pct Recovery = 99%  Analysis Date = 01/17/16 
 Pct Recovery = 99%  Analysis Date = 01/17/16 
 Pct Recovery = 99%  Analysis Date = 01/13/16 
 Pct Recovery = 99%  Analysis Date = 01/13/16 
 Pct Recovery = 99%  Analysis Date = 01/09/16 
 Pct Recovery = 99%  Analysis Date = 01/09/16 
 Pct Recovery = 99%  Analysis Date = 01/05/16 
 Pct Recovery = 99%  Analysis Date = 01/05/16 
 Pct Recovery = 99%  Analysis Date = 01/01/16 
 Pct Recovery = 100%  Analysis Date = 01/01/16 
 Pct Recovery = 100%  Analysis Date = 12/28/15 
 Pct Recovery = 100%  Analysis Date = 12/28/15 
 Pct Recovery = 100%  Analysis Date = 12/24/15 
 Pct Recovery = 100%  Analysis Date = 12/24/15 
 Pct Recovery = 100%  Analysis Date = 12/20/15 
 Pct Recovery = 100%  Analysis Date = 12/20/15 
 Pct Recovery = 100%  Analysis Date = 12/15/15 
 Pct Recovery = 100%  Analysis Date = 12/15/15 
 Pct Recovery = 100%  Analysis Date = 12/11/15 
 Pct Recovery = 100%  Analysis Date = 12/11/15 
 Pct Recovery = 100%  Analysis Date = 12/07/15 
 Pct Recovery = 100%  Analysis Date = 12/07/15 
 Pct Recovery = 100%  Analysis Date = 12/03/15 
 Pct Recovery = 100%  Analysis Date = 12/03/15 
 Pct Recovery = 100%  Analysis Date = 11/29/15 
 Pct Recovery = 101%  Analysis Date = 11/29/15 
 Pct Recovery = 101%  Analysis Date = 11/25/15 
 Pct Recovery = 101%  Analysis Date = 11/25/15 
 Pct Recovery = 101%  Analysis Date = 11/21/15 
 Pct Recovery = 101%  Analysis Date = 11/21/15 
 Pct Recovery = 101%  Analysis Date = 11/16/15 
 Pct Recovery = 101%  Analysis Date = 11/16/15 
 Pct Recovery = 101%  Analysis Date = 11/12/15 
 Pct Recovery = 101%  Analysis Date = 11/12/15 
 Pct Recovery = 101%  Analysis Date = 11/08/15 
 Pct Recovery = 101%  Analysis Date = 11/08/15 
 Pct Recovery = 101%  Analysis Date = 11/04/15 
 Pct Recovery = 101%  Analysis Date = 11/04/15 
 Pct Recovery = 101%  Analysis Date = 10/31/15 
 Pct Recovery = 101%  Analysis Date = 10/31/15 
 Pct Recovery = 101%  Analysis Date = 10/27/15 
 Pct Recovery = 101%  Analysis Date = 10/27/15 
 Pct Recovery = 101%  Analysis Date = 10/23/15 
 Pct Recovery = 101%  Analysis Date = 10/23/15 
 Pct Recovery = 101%  Analysis Date = 10/18/15 
 Pct Recovery = 101%  Analysis Date = 10/18/15 
 Pct Recovery = 101%  Analysis Date = 10/14/15 
 Pct Recovery = 101%  Analysis Date = 10/14/15 
 Pct Recovery = 101%  Analysis Date = 10/10/15 
 Pct Recovery = 101%  Analysis Date = 10/10/15 
 Pct Recovery = 101%  Analysis Date = 10/06/15 
 Pct Recovery = 101%  Analysis Date = 10/06/15 
 Pct Recovery = 101%  Analysis Date = 10/02/15 
 Pct Recovery = 101%  Analysis Date = 10/02/15 
 Pct Recovery = 101%  Analysis Date = 09/28/15 
 Pct Recovery = 101%  Analysis Date = 09/28/15 
 Pct Recovery = 101%  Analysis Date = 09/24/15 
 Pct Recovery = 101%  Analysis Date = 09/24/15 
 Pct Recovery = 101%  Analysis Date = 09/19/15 
 Pct Recovery = 101%  Analysis Date = 09/19/15 
 Pct Recovery = 101%  Analysis Date = 09/15/15 
 Pct Recovery = 101%  Analysis Date = 09/15/15 
 Pct Recovery = 101%  Analysis Date = 09/11/15 
 Pct Recovery = 101%  Analysis Date = 09/11/15 
 Pct Recovery = 101%  Analysis Date = 09/07/15 
 Pct Recovery = 101%  Analysis Date = 09/07/15 
 Pct Recovery = 101%  Analysis Date = 09/03/15 
 Pct Recovery = 101%  Analysis Date = 09/03/15 
 Pct Recovery = 101%  Analysis Date = 08/30/15 
 Pct Recovery = 101%  Analysis Date = 08/30/15 
 Pct Recovery = 101%  Analysis Date = 08/26/15 
 Pct Recovery = 101%  Analysis Date = 08/26/15 
 Pct Recovery = 101%  Analysis Date = 08/21/15 
 Pct Recovery = 101%  Analysis Date = 08/21/15 
 Pct Recovery = 101%  Analysis Date = 08/17/15 
 Pct Recovery = 101%  Analysis Date = 08/17/15 
 Pct Recovery = 101%  Analysis Date = 08/13/15 
 Pct Recovery = 101%  Analysis Date = 08/13/15 
 Pct Recovery = 101%  Analysis Date = 08/09/15 
 Pct Recovery = 101%  Analysis Date = 08/09/15 
 Pct Recovery = 101%  Analysis Date = 08/05/15 
 Pct Recovery = 101%  Analysis Date = 08/05/15 
 Pct Recovery = 101%  Analysis Date = 08/01/15 
 Pct Recovery = 101%  Analysis Date = 08/01/15 
 Pct Recovery = 101%  Analysis Date = 07/28/15 
 Pct Recovery = 101%  Analysis Date = 07/28/15 
 Pct Recovery = 101%  Analysis Date = 07/23/15 
 Pct Recovery = 101%  Analysis Date = 07/23/15 
 Pct Recovery = 101%  Analysis Date = 07/19/15 
 Pct Recovery = 101%  Analysis Date = 07/19/15 
 Pct Recovery = 101%  Analysis Date = 07/15/15 
 Pct Recovery = 101%  Analysis Date = 07/15/15 
 Pct Recovery = 101%  Analysis Date = 07/11/15 
 Pct Recovery = 101%  Analysis Date = 07/11/15 
 Pct Recovery = 101%  Analysis Date = 07/07/15 
 Pct Recovery = 101%  Analysis Date = 07/07/15 
 Pct Recovery = 101%  Analysis Date = 07/03/15 
 Pct Recovery = 101%  Analysis Date = 07/03/15 
 Pct Recovery = 101%  Analysis Date = 06/29/15 
 Pct Recovery = 101%  Analysis Date = 06/29/15 
 Pct Recovery = 101%  Analysis Date = 06/24/15 
 Pct Recovery = 101%  Analysis Date = 06/24/15 
 Pct Recovery = 101%  Analysis Date = 06/20/15 
 Pct Recovery = 101%  Analysis Date = 06/20/15 
 Pct Recovery = 101%  Analysis Date = 06/16/15 
 Pct Recovery = 101%  Analysis Date = 06/16/15 
 Pct Recovery = 101%  Analysis Date = 06/12/15 
 Pct Recovery = 101%  Analysis Date = 06/12/15 
 Pct Recovery = 101%  Analysis Date = 06/08/15 
 Pct Recovery = 101%  Analysis Date = 06/08/15 
 Pct Recovery = 101%  Analysis Date = 06/04/15 
 Pct Recovery = 101%  Analysis Date = 06/04/15 
 Pct Recovery = 101%  Analysis Date = 05/31/15 
 Pct Recovery = 101%  Analysis Date = 05/31/15 
 Pct Recovery = 101%  Analysis Date = 05/27/15 
 Pct Recovery = 101%  Analysis Date = 05/27/15 
 Pct Recovery = 101%  Analysis Date = 05/22/15 
 Pct Recovery = 101%  Analysis Date = 05/22/15 
 Pct Recovery = 101%  Analysis Date = 05/18/15 
 Pct Recovery = 101%  Analysis Date = 05/18/15 
 Pct Recovery = 101%  Analysis Date = 05/14/15 
 Pct Recovery = 101%  Analysis Date = 05/14/15 
 Pct Recovery = 101%  Analysis Date = 05/10/15 
 Pct Recovery = 101%  Analysis Date = 05/10/15 
 Pct Recovery = 101%  Analysis Date = 05/06/15 
 Pct Recovery = 101%  Analysis Date = 05/06/15 
 Pct Recovery = 101%  Analysis Date = 05/02/15 
 Pct Recovery = 101%  Analysis Date = 05/02/15 
 Pct Recovery = 101%  Analysis Date = 04/28/15 
 Pct Recovery = 101%  Analysis Date = 04/28/15 
 Pct Recovery = 101%  Analysis Date = 04/23/15 
 Pct Recovery = 101%  Analysis Date = 04/23/15 
 Pct Recovery = 101%  Analysis Date = 04/19/15 
 Pct Recovery = 101%  Analysis Date = 04/19/15 
 Pct Recovery = 101%  Analysis Date = 04/15/15 
 Pct Recovery = 101%  Analysis Date = 04/15/15 
 Pct Recovery = 101%  Analysis Date = 04/11/15 
 Pct Recovery = 101%  Analysis Date = 04/11/15 
 Pct Recovery = 101%  Analysis Date = 04/07/15 
 Pct Recovery = 101%  Analysis Date = 04/07/15 
 Pct Recovery = 101%  Analysis Date = 04/03/15 
 Pct Recovery = 101%  Analysis Date = 04/03/15 
 Pct Recovery = 101%  Analysis Date = 03/30/15 
 Pct Recovery = 101%  Analysis Date = 03/30/15 
 Pct Recovery = 101%  Analysis Date = 03/25/15 
 Pct Recovery = 101%  Analysis Date = 03/25/15 
 Pct Recovery = 101%  Analysis Date = 03/21/15 
 Pct Recovery = 102%  Analysis Date = 03/21/15 
 Pct Recovery = 102%  Analysis Date = 03/17/15 
 Pct Recovery = 102%  Analysis Date = 03/17/15 
 Pct Recovery = 102%  Analysis Date = 03/13/15 
 Pct Recovery = 102%  Analysis Date = 03/13/15 
 Pct Recovery = 102%  Analysis Date = 03/09/15 
 Pct Recovery = 102%  Analysis Date = 03/09/15 
 Pct Recovery = 102%  Analysis Date = 03/05/15 
 Pct Recovery = 102%  Analysis Date = 03/05/15 
 Pct Recovery = 102%  Analysis Date = 03/01/15 
 Pct Recovery = 102%  Analysis Date = 03/01/15 
 Pct Recovery = 102%  Analysis Date = 02/24/15 
 Pct Recovery = 102%  Analysis Date = 02/24/15 
 Pct Recovery = 102%  Analysis Date = 02/20/15 
 Pct Recovery = 102%  Analysis Date = 02/20/15 
 Pct Recovery = 102%  Analysis Date = 02/16/15 
 Pct Recovery = 102%  Analysis Date = 02/16/15 
 Pct Recovery = 102%  Analysis Date = 02/12/15 
 Pct Recovery = 102%  Analysis Date = 02/12/15 
 Pct Recovery = 102%  Analysis Date = 02/08/15 
 Pct Recovery = 102%  Analysis Date = 02/08/15 
 Pct Recovery = 102%  Analysis Date = 02/04/15 
 Pct Recovery = 102%  Analysis Date = 02/04/15 
 Pct Recovery = 102%  Analysis Date = 01/31/15 
 Pct Recovery = 102%  Analysis Date = 01/31/15 
 Pct Recovery = 102%  Analysis Date = 01/26/15 
 Pct Recovery = 102%  Analysis Date = 01/26/15 
 Pct Recovery = 102%  Analysis Date = 01/22/15 
 Pct Recovery = 102%  Analysis Date = 01/22/15 
 Pct Recovery = 102%  Analysis Date = 01/18/15 
 Pct Recovery = 102%  Analysis Date = 01/18/15 
 Pct Recovery = 102%  Analysis Date = 01/14/15 
 Pct Recovery = 102%  Analysis Date = 01/14/15 
 Pct Recovery = 102%  Analysis Date = 01/10/15 
 Pct Recovery = 102%  Analysis Date = 01/10/15 
 Pct Recovery = 102%  Analysis Date = 01/06/15 
 Pct Recovery = 102%  Analysis Date = 01/06/15 
 Pct Recovery = 102%  Analysis Date = 01/02/15 
 Pct Recovery = 102%  Analysis Date = 01/02/15 
 Pct Recovery = 102%  Analysis Date = 12/28/14 
 Pct Recovery = 103%  Analysis Date = 12/28/14 
 Pct Recovery = 103%  Analysis Date = 12/24/14 
 Pct Recovery = 103%  Analysis Date = 12/24/14 
 Pct Recovery = 103%  Analysis Date = 12/20/14 
 Pct Recovery = 103%  Analysis Date = 12/20/14 
 Pct Recovery = 103%  Analysis Date = 12/16/14 
 Pct Recovery = 103%  Analysis Date = 12/16/14 
 Pct Recovery = 103%  Analysis Date = 12/12/14 
 Pct Recovery = 103%  Analysis Date = 12/12/14 
 Pct Recovery = 103%  Analysis Date = 12/08/14 
 Pct Recovery = 103%  Analysis Date = 12/08/14 
 Pct Recovery = 103%  Analysis Date = 12/04/14 
 Pct Recovery = 103%  Analysis Date = 12/04/14 
 Pct Recovery = 103%  Analysis Date = 11/29/14 
 Pct Recovery = 103%  Analysis Date = 11/29/14 
 Pct Recovery = 103%  Analysis Date = 11/25/14 
 Pct Recovery = 103%  Analysis Date = 11/25/14 
 Pct Recovery = 103%  Analysis Date = 11/21/14 
 Pct Recovery = 103%  Analysis Date = 11/21/14 
 Pct Recovery = 103%  Analysis Date = 11/17/14 
 Pct Recovery = 103%  Analysis Date = 11/17/14 
 Pct Recovery = 103%  Analysis Date = 11/13/14 
 Pct Recovery = 103%  Analysis Date = 11/13/14 
 Pct Recovery = 103%  Analysis Date = 11/09/14 
 Pct Recovery = 103%  Analysis Date = 11/09/14 
 Pct Recovery = 103%  Analysis Date = 11/05/14 
 Pct Recovery = 103%  Analysis Date = 11/05/14 
 Pct Recovery = 103%  Analysis Date = 11/01/14 
 Pct Recovery = 103%  Analysis Date = 11/01/14 
 Pct Recovery = 103%  Analysis Date = 10/27/14 
 Pct Recovery = 103%  Analysis Date = 10/27/14 
 Pct Recovery = 103%  Analysis Date = 10/23/14 
 Pct Recovery = 103%  Analysis Date = 10/23/14 
 Pct Recovery = 103%  Analysis Date = 10/19/14 
 Pct Recovery = 103%  Analysis Date = 10/19/14 
 Pct Recovery = 103%  Analysis Date = 10/15/14 
 Pct Recovery = 103%  Analysis Date = 10/15/14 
 Pct Recovery = 103%  Analysis Date = 10/11/14 
 Pct Recovery = 103%  Analysis Date = 10/11/14 
 Pct Recovery = 103%  Analysis Date = 10/07/14 
 Pct Recovery = 103%  Analysis Date = 10/07/14 
 Pct Recovery = 103%  Analysis Date = 10/03/14 
 Pct Recovery = 103%  Analysis Date = 10/03/14 
 Pct Recovery = 103%  Analysis Date = 09/28/14 
 Pct Recovery = 103%  Analysis Date = 09/28/14 
 Pct Recovery = 103%  Analysis Date = 09/24/14 
 Pct Recovery = 103%  Analysis Date = 09/24/14 
 Pct Recovery = 103%  Analysis Date = 09/20/14 
 Pct Recovery = 103%  Analysis Date = 09/20/14 
 Pct Recovery = 103%  Analysis Date = 09/16/14 
 Pct Recovery = 103%  Analysis Date = 09/16/14 
 Pct Recovery = 103%  Analysis Date = 09/12/14 
 Pct Recovery = 103%  Analysis Date = 09/12/14 
 Pct Recovery = 103%  Analysis Date = 09/08/14 
 Pct Recovery = 103%  Analysis Date = 09/08/14 
 Pct Recovery = 103%  Analysis Date = 09/04/14 
 Pct Recovery = 103%  Analysis Date = 09/04/14 
 Pct Recovery = 103%  Analysis Date = 08/30/14 
 Pct Recovery = 103%  Analysis Date = 08/30/14 
 Pct Recovery = 103%  Analysis Date = 08/26/14 
 Pct Recovery = 103%  Analysis Date = 08/26/14 
 Pct Recovery = 103%  Analysis Date = 08/22/14 
 Pct Recovery = 103%  Analysis Date = 08/22/14 
 Pct Recovery = 103%  Analysis Date = 08/18/14 
 Pct Recovery = 103%  Analysis Date = 08/18/14 
 Pct Recovery = 103%  Analysis Date = 08/14/14 
 Pct Recovery = 103%  Analysis Date = 08/14/14 
 Pct Recovery = 103%  Analysis Date = 08/10/14 
 Pct Recovery = 103%  Analysis Date = 08/10/14 
 Pct Recovery = 103%  Analysis Date = 08/06/14 
 Pct Recovery = 103%  Analysis Date = 08/06/14 
 Pct Recovery = 103%  Analysis Date = 08/01/14 
 Pct Recovery = 103%  Analysis Date = 08/01/14 
 Pct Recovery = 103%  Analysis Date = 07/28/14 
 Pct Recovery = 103%  Analysis Date = 07/28/14 
 Pct Recovery = 103%  Analysis Date = 07/24/14 
 Pct Recovery = 103%  Analysis Date = 07/24/14 
 Pct Recovery = 103%  Analysis Date = 07/20/14 
 Pct Recovery = 103%  Analysis Date = 07/20/14 
 Pct Recovery = 103%  Analysis Date = 07/16/14 
 Pct Recovery = 103%  Analysis Date = 07/16/14 
 Pct Recovery = 103%  Analysis Date = 07/12/14 
 Pct Recovery = 103%  Analysis Date = 07/12/14 
 Pct Recovery = 103%  Analysis Date = 07/08/14 
 Pct Recovery = 103%  Analysis Date = 07/08/14 
 Pct Recovery = 103%  Analysis Date = 07/03/14 
 Pct Recovery = 104%  Analysis Date = 07/03/14 
 Pct Recovery = 104%  Analysis Date = 06/29/14 
 Pct Recovery = 104%  Analysis Date = 06/29/14 
 Pct Recovery = 104%  Analysis Date = 06/25/14 
 Pct Recovery = 104%  Analysis Date = 06/25/14 
 Pct Recovery = 104%  Analysis Date = 06/21/14 
 Pct Recovery = 104%  Analysis Date = 06/21/14 
 Pct Recovery = 104%  Analysis Date = 06/17/14 
 Pct Recovery = 104%  Analysis Date = 06/17/14 
 Pct Recovery = 104%  Analysis Date = 06/13/14 
 Pct Recovery = 104%  Analysis Date = 06/13/14 
 Pct Recovery = 104%  Analysis Date = 06/09/14 
 Pct Recovery = 104%  Analysis Date = 06/09/14 
 Pct Recovery = 104%  Analysis Date = 06/04/14 
 Pct Recovery = 104%  Analysis Date = 06/04/14 
 Pct Recovery = 104%  Analysis Date = 05/31/14 
 Pct Recovery = 104%  Analysis Date = 05/31/14 
 Pct Recovery = 104%  Analysis Date = 05/27/14 
 Pct Recovery = 104%  Analysis Date = 05/27/14 
 Pct Recovery = 104%  Analysis Date = 05/23/14 
 Pct Recovery = 104%  Analysis Date = 05/23/14 
 Pct Recovery = 104%  Analysis Date = 05/19/14 
 Pct Recovery = 104%  Analysis Date = 05/19/14 
 Pct Recovery = 104%  Analysis Date = 05/15/14 
 Pct Recovery = 104%  Analysis Date = 05/15/14 
 Pct Recovery = 104%  Analysis Date = 05/11/14 
 Pct Recovery = 104%  Analysis Date = 05/11/14 
 Pct Recovery = 104%  Analysis Date = 05/07/14 
 Pct Recovery = 104%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
1,2-DIBROMO-3-CHLOROPROPANE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 30 101% 6% 101% 4%
Total 30 101% 6% 101% 4%

Sample Statistics
1,2-DIBROMO-3-CHLOROPROPANE

Characteristic N % % Basis
Plotted 30 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 30 .  
False Negatives 0 0% 0 out of 30
Not Spiked 18 .  
False Positives 0 0% 0 out of 18

BQS OBSP Determination:
1,2-DIBROMOETHANE
METHOD: 4437 , TESTIDCODE: 77651GM016
Open Data Set

 Analysis Date = 06/29/16 
 SpikeMix = NSI 041516: 40 µl & ChemService 5082800: 40 µl 
 Pct Recovery = 100%  Analysis Date = 08/11/16 
 SpikeMix = Phenova B20160303: 25 µl & Supelco LC20145V: 25 µl & NSI 041416HVOC: 25 µl 
 Pct Recovery = 88%  Analysis Date = 01/10/15 
 SpikeMix = Abs 032014: 20 µl & ERA 0321-14-05A: 20 µl 
 Pct Recovery = 91%  Analysis Date = 08/13/14 
 SpikeMix = ERA 0321-14-05: 20 µl & Accu 214031128: 20 µl 
 Pct Recovery = 93%  Analysis Date = 07/11/14 
 SpikeMix = ChemService 2615700: 20 µl & Accu 214031128: 20 µl 
 Pct Recovery = 94%  Analysis Date = 07/03/14 
 SpikeMix = Abs 032014: 20 µl & ChemService 2615700: 20 µl 
 Pct Recovery = 94%  Analysis Date = 06/07/14 
 SpikeMix = ChemService 2615700: 20 µl & Supelco LC06437: 20 µl 
 Pct Recovery = 88%  Analysis Date = 06/06/14 
 SpikeMix = NSI 031814: 20 µl & ChemService 2615700: 20 µl 
 Pct Recovery = 96%  Analysis Date = 07/14/16 
 SpikeMix = NSI 041516: 25 µl & ChemService 5082800: 25 µl & NSI 041416HVOC: 25 µl 
 Pct Recovery = 112%  Analysis Date = 10/09/15 
 SpikeMix = Supelco LC13544: 25 µl & NSI 050515HVOC: 25 µl 
 Pct Recovery = 103%  Analysis Date = 10/09/15 
 SpikeMix = ERA 0601-15-05: 25 µl & Accu 215041338: 25 µl 
 Pct Recovery = 88%  Analysis Date = 06/26/15 
 SpikeMix = ChemService 3818700: 25 µl & Accu 215041338: 25 µl 
 Pct Recovery = 88%  Analysis Date = 07/06/16 
 SpikeMix = Phenova B20160303: 15 µl & Accu 216041354: 15 µl & NSI 041416HVOC: 15 µl 
 Pct Recovery = 77%  Analysis Date = 06/03/16 
 SpikeMix = NSI 041516: 15 µl & Phenova B20160303: 15 µl & NSI 041416HVOC: 15 µl 
 Pct Recovery = 92%  Analysis Date = 07/27/16 
 SpikeMix = ChemService 5082800: 15 µl & Supelco LC20145V: 15 µl & Accu 216041225: 15 µl 
 Pct Recovery = 89%  Analysis Date = 06/23/16 
 SpikeMix = . 
 Pct Recovery = 93%  Analysis Date = 04/28/16 
 SpikeMix = ChemService 3818700: 15 µl & Supelco LC13544: 15 µl 
 Pct Recovery = 109%  Analysis Date = 08/24/15 
 SpikeMix = ERA 0601-15-05: 15 µl & Supelco LC13544: 15 µl 
 Pct Recovery = 106%  Analysis Date = 07/30/15 
 SpikeMix = Supelco LC13544: 15 µl & NSI 050515HVOC: 15 µl 
 Pct Recovery = 98%  Analysis Date = 05/14/15 
 SpikeMix = ChemService 3818700: 15 µl & Supelco LC13544: 15 µl 
 Pct Recovery = 103%  Analysis Date = 11/25/15 
 SpikeMix = Accu 215041338: 15 µl & Abs 040315: 15 µl 
 Pct Recovery = 86%  Analysis Date = 09/05/15 
 SpikeMix = Accu 215041338: 15 µl & NSI 050515HVOC: 15 µl 
 Pct Recovery = 90%  Analysis Date = 04/25/15 
 SpikeMix = Abs 032014: 10 µl & ERA 0321-14-05A: 10 µl 
 Pct Recovery = 104%  Analysis Date = 10/21/14 
 SpikeMix = ERA 0321-14-05A: 10 µl & Accu 214031128: 10 µl 
 Pct Recovery = 105%  Analysis Date = 09/06/14 
 SpikeMix = ERA 0321-14-05: 10 µl & Supelco LC06437: 10 µl 
 Pct Recovery = 99%  Analysis Date = 11/22/14 
 SpikeMix = ChemService 2615700: 10 µl & Supelco LC06437: 10 µl 
 Pct Recovery = 85%  Analysis Date = 07/30/14 
 SpikeMix = NSI 031814: 10 µl & ChemService 2615700: 10 µl 
 Pct Recovery = 105%  Analysis Date = 05/20/14 
 SpikeMix = ChemService 2615700: 10 µl & Accu 214031128: 10 µl 
 Pct Recovery = 96%  Analysis Date = 03/22/16 
 SpikeMix = Supelco LC13544: 10 µl & NSI 050515HVOC: 10 µl 
 Pct Recovery = 102%  Analysis Date = 12/10/15 
 SpikeMix = ChemService 3818700: 10 µl & Supelco LC13544: 10 µl 
 Pct Recovery = 100%  Analysis Date = 05/05/15 
 SpikeMix = Supelco LC13544: 10 µl & Abs 040315: 10 µl 
 Pct Recovery = 110%  Analysis Date = 02/12/16 
 SpikeMix = ERA 0601-15-05: 10 µl & Accu 215041338: 10 µl 
 Pct Recovery = 94%  Analysis Date = 01/05/16 
 SpikeMix = Accu 215041338: 10 µl & Abs 040315: 10 µl 
 Pct Recovery = 108%  Analysis Date = 05/20/15 
 SpikeMix = ChemService 3818700: 10 µl & Accu 215041338: 10 µl 
 Pct Recovery = 84%  Analysis Date = 08/10/16 
 Pct Recovery = 94%  Analysis Date = 08/06/16 
 Pct Recovery = 94%  Analysis Date = 08/06/16 
 Pct Recovery = 94%  Analysis Date = 08/02/16 
 Pct Recovery = 94%  Analysis Date = 08/02/16 
 Pct Recovery = 94%  Analysis Date = 07/29/16 
 Pct Recovery = 94%  Analysis Date = 07/29/16 
 Pct Recovery = 94%  Analysis Date = 07/25/16 
 Pct Recovery = 94%  Analysis Date = 07/25/16 
 Pct Recovery = 94%  Analysis Date = 07/21/16 
 Pct Recovery = 94%  Analysis Date = 07/21/16 
 Pct Recovery = 94%  Analysis Date = 07/17/16 
 Pct Recovery = 95%  Analysis Date = 07/17/16 
 Pct Recovery = 95%  Analysis Date = 07/13/16 
 Pct Recovery = 95%  Analysis Date = 07/13/16 
 Pct Recovery = 95%  Analysis Date = 07/09/16 
 Pct Recovery = 95%  Analysis Date = 07/09/16 
 Pct Recovery = 95%  Analysis Date = 07/05/16 
 Pct Recovery = 95%  Analysis Date = 07/05/16 
 Pct Recovery = 95%  Analysis Date = 07/01/16 
 Pct Recovery = 95%  Analysis Date = 07/01/16 
 Pct Recovery = 95%  Analysis Date = 06/27/16 
 Pct Recovery = 95%  Analysis Date = 06/27/16 
 Pct Recovery = 95%  Analysis Date = 06/23/16 
 Pct Recovery = 95%  Analysis Date = 06/23/16 
 Pct Recovery = 95%  Analysis Date = 06/19/16 
 Pct Recovery = 95%  Analysis Date = 06/19/16 
 Pct Recovery = 95%  Analysis Date = 06/15/16 
 Pct Recovery = 95%  Analysis Date = 06/15/16 
 Pct Recovery = 95%  Analysis Date = 06/10/16 
 Pct Recovery = 95%  Analysis Date = 06/10/16 
 Pct Recovery = 95%  Analysis Date = 06/06/16 
 Pct Recovery = 95%  Analysis Date = 06/06/16 
 Pct Recovery = 95%  Analysis Date = 06/02/16 
 Pct Recovery = 95%  Analysis Date = 06/02/16 
 Pct Recovery = 95%  Analysis Date = 05/29/16 
 Pct Recovery = 95%  Analysis Date = 05/29/16 
 Pct Recovery = 95%  Analysis Date = 05/25/16 
 Pct Recovery = 95%  Analysis Date = 05/25/16 
 Pct Recovery = 95%  Analysis Date = 05/21/16 
 Pct Recovery = 95%  Analysis Date = 05/21/16 
 Pct Recovery = 95%  Analysis Date = 05/17/16 
 Pct Recovery = 96%  Analysis Date = 05/17/16 
 Pct Recovery = 96%  Analysis Date = 05/13/16 
 Pct Recovery = 96%  Analysis Date = 05/13/16 
 Pct Recovery = 96%  Analysis Date = 05/09/16 
 Pct Recovery = 96%  Analysis Date = 05/09/16 
 Pct Recovery = 96%  Analysis Date = 05/05/16 
 Pct Recovery = 96%  Analysis Date = 05/05/16 
 Pct Recovery = 96%  Analysis Date = 05/01/16 
 Pct Recovery = 96%  Analysis Date = 05/01/16 
 Pct Recovery = 96%  Analysis Date = 04/27/16 
 Pct Recovery = 96%  Analysis Date = 04/27/16 
 Pct Recovery = 96%  Analysis Date = 04/23/16 
 Pct Recovery = 96%  Analysis Date = 04/23/16 
 Pct Recovery = 96%  Analysis Date = 04/19/16 
 Pct Recovery = 96%  Analysis Date = 04/19/16 
 Pct Recovery = 96%  Analysis Date = 04/14/16 
 Pct Recovery = 96%  Analysis Date = 04/14/16 
 Pct Recovery = 96%  Analysis Date = 04/10/16 
 Pct Recovery = 96%  Analysis Date = 04/10/16 
 Pct Recovery = 96%  Analysis Date = 04/06/16 
 Pct Recovery = 96%  Analysis Date = 04/06/16 
 Pct Recovery = 96%  Analysis Date = 04/02/16 
 Pct Recovery = 96%  Analysis Date = 04/02/16 
 Pct Recovery = 96%  Analysis Date = 03/29/16 
 Pct Recovery = 96%  Analysis Date = 03/29/16 
 Pct Recovery = 96%  Analysis Date = 03/25/16 
 Pct Recovery = 96%  Analysis Date = 03/25/16 
 Pct Recovery = 96%  Analysis Date = 03/21/16 
 Pct Recovery = 96%  Analysis Date = 03/21/16 
 Pct Recovery = 96%  Analysis Date = 03/17/16 
 Pct Recovery = 96%  Analysis Date = 03/17/16 
 Pct Recovery = 96%  Analysis Date = 03/13/16 
 Pct Recovery = 96%  Analysis Date = 03/13/16 
 Pct Recovery = 96%  Analysis Date = 03/09/16 
 Pct Recovery = 97%  Analysis Date = 03/09/16 
 Pct Recovery = 97%  Analysis Date = 03/05/16 
 Pct Recovery = 97%  Analysis Date = 03/05/16 
 Pct Recovery = 97%  Analysis Date = 03/01/16 
 Pct Recovery = 97%  Analysis Date = 03/01/16 
 Pct Recovery = 97%  Analysis Date = 02/26/16 
 Pct Recovery = 97%  Analysis Date = 02/26/16 
 Pct Recovery = 97%  Analysis Date = 02/22/16 
 Pct Recovery = 97%  Analysis Date = 02/22/16 
 Pct Recovery = 97%  Analysis Date = 02/17/16 
 Pct Recovery = 97%  Analysis Date = 02/17/16 
 Pct Recovery = 97%  Analysis Date = 02/13/16 
 Pct Recovery = 97%  Analysis Date = 02/13/16 
 Pct Recovery = 97%  Analysis Date = 02/09/16 
 Pct Recovery = 97%  Analysis Date = 02/09/16 
 Pct Recovery = 97%  Analysis Date = 02/05/16 
 Pct Recovery = 97%  Analysis Date = 02/05/16 
 Pct Recovery = 97%  Analysis Date = 02/01/16 
 Pct Recovery = 97%  Analysis Date = 02/01/16 
 Pct Recovery = 97%  Analysis Date = 01/28/16 
 Pct Recovery = 97%  Analysis Date = 01/28/16 
 Pct Recovery = 97%  Analysis Date = 01/24/16 
 Pct Recovery = 97%  Analysis Date = 01/24/16 
 Pct Recovery = 97%  Analysis Date = 01/20/16 
 Pct Recovery = 97%  Analysis Date = 01/20/16 
 Pct Recovery = 97%  Analysis Date = 01/16/16 
 Pct Recovery = 97%  Analysis Date = 01/16/16 
 Pct Recovery = 97%  Analysis Date = 01/12/16 
 Pct Recovery = 97%  Analysis Date = 01/12/16 
 Pct Recovery = 97%  Analysis Date = 01/08/16 
 Pct Recovery = 97%  Analysis Date = 01/08/16 
 Pct Recovery = 97%  Analysis Date = 01/04/16 
 Pct Recovery = 97%  Analysis Date = 01/04/16 
 Pct Recovery = 97%  Analysis Date = 12/31/15 
 Pct Recovery = 97%  Analysis Date = 12/31/15 
 Pct Recovery = 97%  Analysis Date = 12/27/15 
 Pct Recovery = 97%  Analysis Date = 12/27/15 
 Pct Recovery = 97%  Analysis Date = 12/23/15 
 Pct Recovery = 97%  Analysis Date = 12/23/15 
 Pct Recovery = 97%  Analysis Date = 12/18/15 
 Pct Recovery = 97%  Analysis Date = 12/18/15 
 Pct Recovery = 97%  Analysis Date = 12/14/15 
 Pct Recovery = 97%  Analysis Date = 12/14/15 
 Pct Recovery = 97%  Analysis Date = 12/10/15 
 Pct Recovery = 97%  Analysis Date = 12/10/15 
 Pct Recovery = 97%  Analysis Date = 12/06/15 
 Pct Recovery = 97%  Analysis Date = 12/06/15 
 Pct Recovery = 97%  Analysis Date = 12/02/15 
 Pct Recovery = 97%  Analysis Date = 12/02/15 
 Pct Recovery = 97%  Analysis Date = 11/28/15 
 Pct Recovery = 97%  Analysis Date = 11/28/15 
 Pct Recovery = 97%  Analysis Date = 11/24/15 
 Pct Recovery = 97%  Analysis Date = 11/24/15 
 Pct Recovery = 97%  Analysis Date = 11/20/15 
 Pct Recovery = 97%  Analysis Date = 11/20/15 
 Pct Recovery = 97%  Analysis Date = 11/16/15 
 Pct Recovery = 97%  Analysis Date = 11/16/15 
 Pct Recovery = 97%  Analysis Date = 11/12/15 
 Pct Recovery = 97%  Analysis Date = 11/12/15 
 Pct Recovery = 97%  Analysis Date = 11/08/15 
 Pct Recovery = 97%  Analysis Date = 11/08/15 
 Pct Recovery = 97%  Analysis Date = 11/04/15 
 Pct Recovery = 97%  Analysis Date = 11/04/15 
 Pct Recovery = 97%  Analysis Date = 10/31/15 
 Pct Recovery = 97%  Analysis Date = 10/31/15 
 Pct Recovery = 97%  Analysis Date = 10/27/15 
 Pct Recovery = 97%  Analysis Date = 10/27/15 
 Pct Recovery = 97%  Analysis Date = 10/22/15 
 Pct Recovery = 97%  Analysis Date = 10/22/15 
 Pct Recovery = 97%  Analysis Date = 10/18/15 
 Pct Recovery = 97%  Analysis Date = 10/18/15 
 Pct Recovery = 97%  Analysis Date = 10/14/15 
 Pct Recovery = 97%  Analysis Date = 10/14/15 
 Pct Recovery = 97%  Analysis Date = 10/10/15 
 Pct Recovery = 97%  Analysis Date = 10/10/15 
 Pct Recovery = 97%  Analysis Date = 10/06/15 
 Pct Recovery = 97%  Analysis Date = 10/06/15 
 Pct Recovery = 97%  Analysis Date = 10/02/15 
 Pct Recovery = 97%  Analysis Date = 10/02/15 
 Pct Recovery = 97%  Analysis Date = 09/28/15 
 Pct Recovery = 97%  Analysis Date = 09/28/15 
 Pct Recovery = 97%  Analysis Date = 09/24/15 
 Pct Recovery = 97%  Analysis Date = 09/24/15 
 Pct Recovery = 97%  Analysis Date = 09/20/15 
 Pct Recovery = 97%  Analysis Date = 09/20/15 
 Pct Recovery = 97%  Analysis Date = 09/16/15 
 Pct Recovery = 97%  Analysis Date = 09/16/15 
 Pct Recovery = 97%  Analysis Date = 09/12/15 
 Pct Recovery = 97%  Analysis Date = 09/12/15 
 Pct Recovery = 97%  Analysis Date = 09/08/15 
 Pct Recovery = 97%  Analysis Date = 09/08/15 
 Pct Recovery = 97%  Analysis Date = 09/04/15 
 Pct Recovery = 97%  Analysis Date = 09/04/15 
 Pct Recovery = 97%  Analysis Date = 08/31/15 
 Pct Recovery = 97%  Analysis Date = 08/31/15 
 Pct Recovery = 97%  Analysis Date = 08/26/15 
 Pct Recovery = 97%  Analysis Date = 08/26/15 
 Pct Recovery = 97%  Analysis Date = 08/22/15 
 Pct Recovery = 97%  Analysis Date = 08/22/15 
 Pct Recovery = 97%  Analysis Date = 08/18/15 
 Pct Recovery = 97%  Analysis Date = 08/18/15 
 Pct Recovery = 97%  Analysis Date = 08/14/15 
 Pct Recovery = 97%  Analysis Date = 08/14/15 
 Pct Recovery = 97%  Analysis Date = 08/10/15 
 Pct Recovery = 97%  Analysis Date = 08/10/15 
 Pct Recovery = 97%  Analysis Date = 08/06/15 
 Pct Recovery = 97%  Analysis Date = 08/06/15 
 Pct Recovery = 97%  Analysis Date = 08/02/15 
 Pct Recovery = 97%  Analysis Date = 08/02/15 
 Pct Recovery = 97%  Analysis Date = 07/29/15 
 Pct Recovery = 97%  Analysis Date = 07/29/15 
 Pct Recovery = 97%  Analysis Date = 07/25/15 
 Pct Recovery = 97%  Analysis Date = 07/25/15 
 Pct Recovery = 97%  Analysis Date = 07/21/15 
 Pct Recovery = 97%  Analysis Date = 07/21/15 
 Pct Recovery = 97%  Analysis Date = 07/17/15 
 Pct Recovery = 97%  Analysis Date = 07/17/15 
 Pct Recovery = 97%  Analysis Date = 07/13/15 
 Pct Recovery = 97%  Analysis Date = 07/13/15 
 Pct Recovery = 97%  Analysis Date = 07/09/15 
 Pct Recovery = 97%  Analysis Date = 07/09/15 
 Pct Recovery = 97%  Analysis Date = 07/05/15 
 Pct Recovery = 97%  Analysis Date = 07/05/15 
 Pct Recovery = 97%  Analysis Date = 06/30/15 
 Pct Recovery = 97%  Analysis Date = 06/30/15 
 Pct Recovery = 97%  Analysis Date = 06/26/15 
 Pct Recovery = 97%  Analysis Date = 06/26/15 
 Pct Recovery = 97%  Analysis Date = 06/22/15 
 Pct Recovery = 97%  Analysis Date = 06/22/15 
 Pct Recovery = 97%  Analysis Date = 06/18/15 
 Pct Recovery = 97%  Analysis Date = 06/18/15 
 Pct Recovery = 97%  Analysis Date = 06/14/15 
 Pct Recovery = 97%  Analysis Date = 06/14/15 
 Pct Recovery = 97%  Analysis Date = 06/10/15 
 Pct Recovery = 97%  Analysis Date = 06/10/15 
 Pct Recovery = 97%  Analysis Date = 06/06/15 
 Pct Recovery = 97%  Analysis Date = 06/06/15 
 Pct Recovery = 97%  Analysis Date = 06/02/15 
 Pct Recovery = 97%  Analysis Date = 06/02/15 
 Pct Recovery = 97%  Analysis Date = 05/29/15 
 Pct Recovery = 97%  Analysis Date = 05/29/15 
 Pct Recovery = 97%  Analysis Date = 05/25/15 
 Pct Recovery = 97%  Analysis Date = 05/25/15 
 Pct Recovery = 97%  Analysis Date = 05/21/15 
 Pct Recovery = 97%  Analysis Date = 05/21/15 
 Pct Recovery = 97%  Analysis Date = 05/17/15 
 Pct Recovery = 96%  Analysis Date = 05/17/15 
 Pct Recovery = 96%  Analysis Date = 05/13/15 
 Pct Recovery = 96%  Analysis Date = 05/13/15 
 Pct Recovery = 96%  Analysis Date = 05/09/15 
 Pct Recovery = 96%  Analysis Date = 05/09/15 
 Pct Recovery = 96%  Analysis Date = 05/05/15 
 Pct Recovery = 96%  Analysis Date = 05/05/15 
 Pct Recovery = 96%  Analysis Date = 04/30/15 
 Pct Recovery = 96%  Analysis Date = 04/30/15 
 Pct Recovery = 96%  Analysis Date = 04/26/15 
 Pct Recovery = 96%  Analysis Date = 04/26/15 
 Pct Recovery = 96%  Analysis Date = 04/22/15 
 Pct Recovery = 96%  Analysis Date = 04/22/15 
 Pct Recovery = 96%  Analysis Date = 04/18/15 
 Pct Recovery = 96%  Analysis Date = 04/18/15 
 Pct Recovery = 96%  Analysis Date = 04/14/15 
 Pct Recovery = 96%  Analysis Date = 04/14/15 
 Pct Recovery = 96%  Analysis Date = 04/10/15 
 Pct Recovery = 96%  Analysis Date = 04/10/15 
 Pct Recovery = 96%  Analysis Date = 04/06/15 
 Pct Recovery = 96%  Analysis Date = 04/06/15 
 Pct Recovery = 96%  Analysis Date = 04/02/15 
 Pct Recovery = 96%  Analysis Date = 04/02/15 
 Pct Recovery = 96%  Analysis Date = 03/29/15 
 Pct Recovery = 96%  Analysis Date = 03/29/15 
 Pct Recovery = 96%  Analysis Date = 03/25/15 
 Pct Recovery = 96%  Analysis Date = 03/25/15 
 Pct Recovery = 96%  Analysis Date = 03/21/15 
 Pct Recovery = 96%  Analysis Date = 03/21/15 
 Pct Recovery = 96%  Analysis Date = 03/17/15 
 Pct Recovery = 96%  Analysis Date = 03/17/15 
 Pct Recovery = 96%  Analysis Date = 03/13/15 
 Pct Recovery = 96%  Analysis Date = 03/13/15 
 Pct Recovery = 96%  Analysis Date = 03/09/15 
 Pct Recovery = 96%  Analysis Date = 03/09/15 
 Pct Recovery = 96%  Analysis Date = 03/04/15 
 Pct Recovery = 96%  Analysis Date = 03/04/15 
 Pct Recovery = 96%  Analysis Date = 02/28/15 
 Pct Recovery = 96%  Analysis Date = 02/28/15 
 Pct Recovery = 96%  Analysis Date = 02/24/15 
 Pct Recovery = 96%  Analysis Date = 02/24/15 
 Pct Recovery = 96%  Analysis Date = 02/20/15 
 Pct Recovery = 96%  Analysis Date = 02/20/15 
 Pct Recovery = 96%  Analysis Date = 02/16/15 
 Pct Recovery = 96%  Analysis Date = 02/16/15 
 Pct Recovery = 96%  Analysis Date = 02/12/15 
 Pct Recovery = 96%  Analysis Date = 02/12/15 
 Pct Recovery = 96%  Analysis Date = 02/08/15 
 Pct Recovery = 96%  Analysis Date = 02/08/15 
 Pct Recovery = 96%  Analysis Date = 02/04/15 
 Pct Recovery = 96%  Analysis Date = 02/04/15 
 Pct Recovery = 96%  Analysis Date = 01/31/15 
 Pct Recovery = 96%  Analysis Date = 01/31/15 
 Pct Recovery = 96%  Analysis Date = 01/27/15 
 Pct Recovery = 96%  Analysis Date = 01/27/15 
 Pct Recovery = 96%  Analysis Date = 01/23/15 
 Pct Recovery = 96%  Analysis Date = 01/23/15 
 Pct Recovery = 96%  Analysis Date = 01/19/15 
 Pct Recovery = 96%  Analysis Date = 01/19/15 
 Pct Recovery = 96%  Analysis Date = 01/15/15 
 Pct Recovery = 96%  Analysis Date = 01/15/15 
 Pct Recovery = 96%  Analysis Date = 01/11/15 
 Pct Recovery = 96%  Analysis Date = 01/11/15 
 Pct Recovery = 96%  Analysis Date = 01/06/15 
 Pct Recovery = 96%  Analysis Date = 01/06/15 
 Pct Recovery = 96%  Analysis Date = 01/02/15 
 Pct Recovery = 96%  Analysis Date = 01/02/15 
 Pct Recovery = 96%  Analysis Date = 12/29/14 
 Pct Recovery = 96%  Analysis Date = 12/29/14 
 Pct Recovery = 96%  Analysis Date = 12/25/14 
 Pct Recovery = 96%  Analysis Date = 12/25/14 
 Pct Recovery = 96%  Analysis Date = 12/21/14 
 Pct Recovery = 96%  Analysis Date = 12/21/14 
 Pct Recovery = 96%  Analysis Date = 12/17/14 
 Pct Recovery = 96%  Analysis Date = 12/17/14 
 Pct Recovery = 96%  Analysis Date = 12/13/14 
 Pct Recovery = 96%  Analysis Date = 12/13/14 
 Pct Recovery = 96%  Analysis Date = 12/09/14 
 Pct Recovery = 96%  Analysis Date = 12/09/14 
 Pct Recovery = 96%  Analysis Date = 12/05/14 
 Pct Recovery = 96%  Analysis Date = 12/05/14 
 Pct Recovery = 96%  Analysis Date = 12/01/14 
 Pct Recovery = 96%  Analysis Date = 12/01/14 
 Pct Recovery = 96%  Analysis Date = 11/27/14 
 Pct Recovery = 96%  Analysis Date = 11/27/14 
 Pct Recovery = 96%  Analysis Date = 11/23/14 
 Pct Recovery = 96%  Analysis Date = 11/23/14 
 Pct Recovery = 96%  Analysis Date = 11/19/14 
 Pct Recovery = 96%  Analysis Date = 11/19/14 
 Pct Recovery = 96%  Analysis Date = 11/15/14 
 Pct Recovery = 96%  Analysis Date = 11/15/14 
 Pct Recovery = 96%  Analysis Date = 11/11/14 
 Pct Recovery = 96%  Analysis Date = 11/11/14 
 Pct Recovery = 96%  Analysis Date = 11/06/14 
 Pct Recovery = 96%  Analysis Date = 11/06/14 
 Pct Recovery = 96%  Analysis Date = 11/02/14 
 Pct Recovery = 96%  Analysis Date = 11/02/14 
 Pct Recovery = 96%  Analysis Date = 10/29/14 
 Pct Recovery = 96%  Analysis Date = 10/29/14 
 Pct Recovery = 96%  Analysis Date = 10/25/14 
 Pct Recovery = 96%  Analysis Date = 10/25/14 
 Pct Recovery = 96%  Analysis Date = 10/21/14 
 Pct Recovery = 96%  Analysis Date = 10/21/14 
 Pct Recovery = 96%  Analysis Date = 10/17/14 
 Pct Recovery = 96%  Analysis Date = 10/17/14 
 Pct Recovery = 96%  Analysis Date = 10/13/14 
 Pct Recovery = 96%  Analysis Date = 10/13/14 
 Pct Recovery = 96%  Analysis Date = 10/09/14 
 Pct Recovery = 96%  Analysis Date = 10/09/14 
 Pct Recovery = 96%  Analysis Date = 10/05/14 
 Pct Recovery = 96%  Analysis Date = 10/05/14 
 Pct Recovery = 96%  Analysis Date = 10/01/14 
 Pct Recovery = 96%  Analysis Date = 10/01/14 
 Pct Recovery = 96%  Analysis Date = 09/27/14 
 Pct Recovery = 96%  Analysis Date = 09/27/14 
 Pct Recovery = 96%  Analysis Date = 09/23/14 
 Pct Recovery = 96%  Analysis Date = 09/23/14 
 Pct Recovery = 96%  Analysis Date = 09/19/14 
 Pct Recovery = 96%  Analysis Date = 09/19/14 
 Pct Recovery = 96%  Analysis Date = 09/15/14 
 Pct Recovery = 96%  Analysis Date = 09/15/14 
 Pct Recovery = 96%  Analysis Date = 09/10/14 
 Pct Recovery = 96%  Analysis Date = 09/10/14 
 Pct Recovery = 96%  Analysis Date = 09/06/14 
 Pct Recovery = 96%  Analysis Date = 09/06/14 
 Pct Recovery = 96%  Analysis Date = 09/02/14 
 Pct Recovery = 96%  Analysis Date = 09/02/14 
 Pct Recovery = 96%  Analysis Date = 08/29/14 
 Pct Recovery = 96%  Analysis Date = 08/29/14 
 Pct Recovery = 96%  Analysis Date = 08/25/14 
 Pct Recovery = 96%  Analysis Date = 08/25/14 
 Pct Recovery = 96%  Analysis Date = 08/21/14 
 Pct Recovery = 96%  Analysis Date = 08/21/14 
 Pct Recovery = 96%  Analysis Date = 08/17/14 
 Pct Recovery = 96%  Analysis Date = 08/17/14 
 Pct Recovery = 96%  Analysis Date = 08/13/14 
 Pct Recovery = 96%  Analysis Date = 08/13/14 
 Pct Recovery = 96%  Analysis Date = 08/09/14 
 Pct Recovery = 96%  Analysis Date = 08/09/14 
 Pct Recovery = 96%  Analysis Date = 08/05/14 
 Pct Recovery = 96%  Analysis Date = 08/05/14 
 Pct Recovery = 96%  Analysis Date = 08/01/14 
 Pct Recovery = 95%  Analysis Date = 08/01/14 
 Pct Recovery = 95%  Analysis Date = 07/28/14 
 Pct Recovery = 95%  Analysis Date = 07/28/14 
 Pct Recovery = 95%  Analysis Date = 07/24/14 
 Pct Recovery = 95%  Analysis Date = 07/24/14 
 Pct Recovery = 95%  Analysis Date = 07/20/14 
 Pct Recovery = 95%  Analysis Date = 07/20/14 
 Pct Recovery = 95%  Analysis Date = 07/15/14 
 Pct Recovery = 95%  Analysis Date = 07/15/14 
 Pct Recovery = 95%  Analysis Date = 07/11/14 
 Pct Recovery = 95%  Analysis Date = 07/11/14 
 Pct Recovery = 95%  Analysis Date = 07/07/14 
 Pct Recovery = 95%  Analysis Date = 07/07/14 
 Pct Recovery = 95%  Analysis Date = 07/03/14 
 Pct Recovery = 95%  Analysis Date = 07/03/14 
 Pct Recovery = 95%  Analysis Date = 06/29/14 
 Pct Recovery = 95%  Analysis Date = 06/29/14 
 Pct Recovery = 95%  Analysis Date = 06/25/14 
 Pct Recovery = 95%  Analysis Date = 06/25/14 
 Pct Recovery = 95%  Analysis Date = 06/21/14 
 Pct Recovery = 95%  Analysis Date = 06/21/14 
 Pct Recovery = 95%  Analysis Date = 06/17/14 
 Pct Recovery = 95%  Analysis Date = 06/17/14 
 Pct Recovery = 95%  Analysis Date = 06/13/14 
 Pct Recovery = 95%  Analysis Date = 06/13/14 
 Pct Recovery = 95%  Analysis Date = 06/09/14 
 Pct Recovery = 95%  Analysis Date = 06/09/14 
 Pct Recovery = 95%  Analysis Date = 06/05/14 
 Pct Recovery = 95%  Analysis Date = 06/05/14 
 Pct Recovery = 95%  Analysis Date = 06/01/14 
 Pct Recovery = 95%  Analysis Date = 06/01/14 
 Pct Recovery = 95%  Analysis Date = 05/28/14 
 Pct Recovery = 95%  Analysis Date = 05/28/14 
 Pct Recovery = 95%  Analysis Date = 05/24/14 
 Pct Recovery = 95%  Analysis Date = 05/24/14 
 Pct Recovery = 95%  Analysis Date = 05/20/14 
 Pct Recovery = 95%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
1,2-DIBROMOETHANE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 34 96% 8% 95% 11%
Total 34 96% 8% 95% 11%

Sample Statistics
1,2-DIBROMOETHANE

Characteristic N % % Basis
Plotted 34 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 34 .  
False Negatives 0 0% 0 out of 34
Not Spiked 21 .  
False Positives 0 0% 0 out of 21

BQS OBSP Determination:
1,2-DICHLOROPROPANE
METHOD: 4437 , TESTIDCODE: 34541GM016
Open Data Set

 Analysis Date = 07/29/16 
 SpikeMix = Supelco LC20145V: 40 µl & NSI 041516: 40 µl & NSI 041416HVOC: 40 µl 
 Pct Recovery = 109%  Analysis Date = 07/06/16 
 SpikeMix = Accu 216041354: 40 µl & NSI 041516: 40 µl & NSI 041416HVOC: 40 µl 
 Pct Recovery = 112%  Analysis Date = 03/19/15 
 SpikeMix = Supelco LC06437: 20 µl & NSI 031814: 20 µl 
 Pct Recovery = 111%  Analysis Date = 01/10/15 
 SpikeMix = Abs 032014: 20 µl & ERA 0321-14-05A: 20 µl 
 Pct Recovery = 96%  Analysis Date = 08/20/14 
 SpikeMix = Supelco LC06437: 20 µl & Abs 032014: 20 µl 
 Pct Recovery = 88%  Analysis Date = 07/23/14 
 SpikeMix = Accu 214031128: 20 µl & Abs 032014: 20 µl 
 Pct Recovery = 91%  Analysis Date = 07/03/14 
 SpikeMix = Abs 032014: 20 µl & ChemService 2615700: 20 µl 
 Pct Recovery = 99%  Analysis Date = 06/06/14 
 SpikeMix = NSI 031814: 20 µl & ChemService 2615700: 20 µl 
 Pct Recovery = 116%  Analysis Date = 05/07/14 
 SpikeMix = NSI 031814: 20 µl & Accu 214031128: 20 µl 
 Pct Recovery = 109%  Analysis Date = 08/11/16 
 SpikeMix = Phenova B20160303: 25 µl & Supelco LC20145V: 25 µl & NSI 041416HVOC: 25 µl 
 Pct Recovery = 99%  Analysis Date = 05/21/16 
 SpikeMix = Supelco LC20145V: 25 µl & NSI 041516: 25 µl & NSI 041416HVOC: 25 µl 
 Pct Recovery = 110%  Analysis Date = 06/26/15 
 SpikeMix = ChemService 3818700: 25 µl & Accu 215041338: 25 µl 
 Pct Recovery = 103%  Analysis Date = 06/25/15 
 SpikeMix = ChemService 3818700: 25 µl & NSI 050515HVOC: 25 µl 
 Pct Recovery = 103%  Analysis Date = 01/22/16 
 SpikeMix = NSI 050515HVOC: 25 µl & ERA 0601-15-05: 25 µl 
 Pct Recovery = 95%  Analysis Date = 10/09/15 
 SpikeMix = ERA 0601-15-05: 25 µl & Accu 215041338: 25 µl 
 Pct Recovery = 109%  Analysis Date = 08/12/16 
 SpikeMix = Accu 216041354: 15 µl & Abs 060916HVOC: 15 µl 
 Pct Recovery = 94%  Analysis Date = 07/27/16 
 SpikeMix = ChemService 5082800: 15 µl & Supelco LC20145V: 15 µl & Accu 216041225: 15 µl 
 Pct Recovery = 106%  Analysis Date = 07/06/16 
 SpikeMix = Phenova B20160303: 15 µl & Accu 216041354: 15 µl & NSI 041416HVOC: 15 µl 
 Pct Recovery = 113%  Analysis Date = 06/23/16 
 SpikeMix = . 
 Pct Recovery = 97%  Analysis Date = 05/20/16 
 SpikeMix = Accu 216041354: 15 µl & NSI 041516: 15 µl & Accu 216041225: 15 µl 
 Pct Recovery = 104%  Analysis Date = 04/28/16 
 SpikeMix = ChemService 3818700: 15 µl & Supelco LC13544: 15 µl 
 Pct Recovery = 102%  Analysis Date = 06/16/15 
 SpikeMix = ChemService 3818700: 15 µl & NSI 050515HVOC: 15 µl 
 Pct Recovery = 101%  Analysis Date = 05/14/15 
 SpikeMix = ChemService 3818700: 15 µl & Supelco LC13544: 15 µl 
 Pct Recovery = 104%  Analysis Date = 09/24/15 
 SpikeMix = Abs 040315: 15 µl & ERA 0601-15-05: 15 µl 
 Pct Recovery = 102%  Analysis Date = 08/24/15 
 SpikeMix = ERA 0601-15-05: 15 µl & Supelco LC13544: 15 µl 
 Pct Recovery = 89%  Analysis Date = 04/25/15 
 SpikeMix = Abs 032014: 10 µl & ERA 0321-14-05A: 10 µl 
 Pct Recovery = 100%  Analysis Date = 12/13/14 
 SpikeMix = Accu 214031128: 10 µl & NSI 031814: 10 µl 
 Pct Recovery = 109%  Analysis Date = 09/11/14 
 SpikeMix = Accu 214031128: 10 µl & Abs 032014: 10 µl 
 Pct Recovery = 115%  Analysis Date = 07/30/14 
 SpikeMix = NSI 031814: 10 µl & ChemService 2615700: 10 µl 
 Pct Recovery = 109%  Analysis Date = 06/17/14 
 SpikeMix = Supelco LC06437: 10 µl & Abs 032014: 10 µl 
 Pct Recovery = 99%  Analysis Date = 04/09/16 
 SpikeMix = Abs 040315: 10 µl & ChemService 3818700: 10 µl 
 Pct Recovery = 110%  Analysis Date = 12/10/15 
 SpikeMix = ChemService 3818700: 10 µl & Supelco LC13544: 10 µl 
 Pct Recovery = 90%  Analysis Date = 10/23/15 
 SpikeMix = Abs 040315: 10 µl & ChemService 3818700: 10 µl 
 Pct Recovery = 112%  Analysis Date = 05/20/15 
 SpikeMix = ChemService 3818700: 10 µl & Accu 215041338: 10 µl 
 Pct Recovery = 107%  Analysis Date = 02/12/16 
 SpikeMix = ERA 0601-15-05: 10 µl & Accu 215041338: 10 µl 
 Pct Recovery = 99%  Analysis Date = 12/05/15 
 SpikeMix = NSI 050515HVOC: 10 µl & ERA 0601-15-05: 10 µl 
 Pct Recovery = 91%  Analysis Date = 11/14/15 
 SpikeMix = ERA 0601-15-05: 10 µl 
 Pct Recovery = 97%  Analysis Date = 08/14/15 
 SpikeMix = Abs 040315: 10 µl & ERA 0601-15-05: 10 µl 
 Pct Recovery = 87%  Analysis Date = 08/11/16 
 Pct Recovery = 106%  Analysis Date = 08/07/16 
 Pct Recovery = 105%  Analysis Date = 08/07/16 
 Pct Recovery = 105%  Analysis Date = 08/03/16 
 Pct Recovery = 105%  Analysis Date = 08/03/16 
 Pct Recovery = 105%  Analysis Date = 07/30/16 
 Pct Recovery = 105%  Analysis Date = 07/30/16 
 Pct Recovery = 105%  Analysis Date = 07/26/16 
 Pct Recovery = 105%  Analysis Date = 07/26/16 
 Pct Recovery = 105%  Analysis Date = 07/22/16 
 Pct Recovery = 105%  Analysis Date = 07/22/16 
 Pct Recovery = 105%  Analysis Date = 07/18/16 
 Pct Recovery = 105%  Analysis Date = 07/18/16 
 Pct Recovery = 105%  Analysis Date = 07/14/16 
 Pct Recovery = 105%  Analysis Date = 07/14/16 
 Pct Recovery = 105%  Analysis Date = 07/09/16 
 Pct Recovery = 105%  Analysis Date = 07/09/16 
 Pct Recovery = 105%  Analysis Date = 07/05/16 
 Pct Recovery = 105%  Analysis Date = 07/05/16 
 Pct Recovery = 105%  Analysis Date = 07/01/16 
 Pct Recovery = 105%  Analysis Date = 07/01/16 
 Pct Recovery = 105%  Analysis Date = 06/27/16 
 Pct Recovery = 104%  Analysis Date = 06/27/16 
 Pct Recovery = 104%  Analysis Date = 06/23/16 
 Pct Recovery = 104%  Analysis Date = 06/23/16 
 Pct Recovery = 104%  Analysis Date = 06/19/16 
 Pct Recovery = 104%  Analysis Date = 06/19/16 
 Pct Recovery = 104%  Analysis Date = 06/15/16 
 Pct Recovery = 104%  Analysis Date = 06/15/16 
 Pct Recovery = 104%  Analysis Date = 06/10/16 
 Pct Recovery = 104%  Analysis Date = 06/10/16 
 Pct Recovery = 104%  Analysis Date = 06/06/16 
 Pct Recovery = 104%  Analysis Date = 06/06/16 
 Pct Recovery = 104%  Analysis Date = 06/02/16 
 Pct Recovery = 104%  Analysis Date = 06/02/16 
 Pct Recovery = 104%  Analysis Date = 05/29/16 
 Pct Recovery = 104%  Analysis Date = 05/29/16 
 Pct Recovery = 104%  Analysis Date = 05/25/16 
 Pct Recovery = 104%  Analysis Date = 05/25/16 
 Pct Recovery = 104%  Analysis Date = 05/21/16 
 Pct Recovery = 103%  Analysis Date = 05/21/16 
 Pct Recovery = 103%  Analysis Date = 05/17/16 
 Pct Recovery = 103%  Analysis Date = 05/17/16 
 Pct Recovery = 103%  Analysis Date = 05/12/16 
 Pct Recovery = 103%  Analysis Date = 05/12/16 
 Pct Recovery = 103%  Analysis Date = 05/08/16 
 Pct Recovery = 103%  Analysis Date = 05/08/16 
 Pct Recovery = 103%  Analysis Date = 05/04/16 
 Pct Recovery = 103%  Analysis Date = 05/04/16 
 Pct Recovery = 103%  Analysis Date = 04/30/16 
 Pct Recovery = 103%  Analysis Date = 04/30/16 
 Pct Recovery = 103%  Analysis Date = 04/26/16 
 Pct Recovery = 103%  Analysis Date = 04/26/16 
 Pct Recovery = 103%  Analysis Date = 04/22/16 
 Pct Recovery = 103%  Analysis Date = 04/22/16 
 Pct Recovery = 103%  Analysis Date = 04/18/16 
 Pct Recovery = 103%  Analysis Date = 04/18/16 
 Pct Recovery = 103%  Analysis Date = 04/13/16 
 Pct Recovery = 103%  Analysis Date = 04/13/16 
 Pct Recovery = 103%  Analysis Date = 04/09/16 
 Pct Recovery = 102%  Analysis Date = 04/09/16 
 Pct Recovery = 102%  Analysis Date = 04/05/16 
 Pct Recovery = 102%  Analysis Date = 04/05/16 
 Pct Recovery = 102%  Analysis Date = 04/01/16 
 Pct Recovery = 102%  Analysis Date = 04/01/16 
 Pct Recovery = 102%  Analysis Date = 03/28/16 
 Pct Recovery = 102%  Analysis Date = 03/28/16 
 Pct Recovery = 102%  Analysis Date = 03/24/16 
 Pct Recovery = 102%  Analysis Date = 03/24/16 
 Pct Recovery = 102%  Analysis Date = 03/20/16 
 Pct Recovery = 102%  Analysis Date = 03/20/16 
 Pct Recovery = 102%  Analysis Date = 03/15/16 
 Pct Recovery = 102%  Analysis Date = 03/15/16 
 Pct Recovery = 102%  Analysis Date = 03/11/16 
 Pct Recovery = 102%  Analysis Date = 03/11/16 
 Pct Recovery = 102%  Analysis Date = 03/07/16 
 Pct Recovery = 102%  Analysis Date = 03/07/16 
 Pct Recovery = 102%  Analysis Date = 03/03/16 
 Pct Recovery = 102%  Analysis Date = 03/03/16 
 Pct Recovery = 102%  Analysis Date = 02/28/16 
 Pct Recovery = 102%  Analysis Date = 02/28/16 
 Pct Recovery = 102%  Analysis Date = 02/24/16 
 Pct Recovery = 101%  Analysis Date = 02/24/16 
 Pct Recovery = 101%  Analysis Date = 02/20/16 
 Pct Recovery = 101%  Analysis Date = 02/20/16 
 Pct Recovery = 101%  Analysis Date = 02/15/16 
 Pct Recovery = 101%  Analysis Date = 02/15/16 
 Pct Recovery = 101%  Analysis Date = 02/11/16 
 Pct Recovery = 101%  Analysis Date = 02/11/16 
 Pct Recovery = 101%  Analysis Date = 02/07/16 
 Pct Recovery = 101%  Analysis Date = 02/07/16 
 Pct Recovery = 101%  Analysis Date = 02/03/16 
 Pct Recovery = 101%  Analysis Date = 02/03/16 
 Pct Recovery = 101%  Analysis Date = 01/30/16 
 Pct Recovery = 101%  Analysis Date = 01/30/16 
 Pct Recovery = 101%  Analysis Date = 01/26/16 
 Pct Recovery = 101%  Analysis Date = 01/26/16 
 Pct Recovery = 101%  Analysis Date = 01/22/16 
 Pct Recovery = 101%  Analysis Date = 01/22/16 
 Pct Recovery = 101%  Analysis Date = 01/17/16 
 Pct Recovery = 100%  Analysis Date = 01/17/16 
 Pct Recovery = 100%  Analysis Date = 01/13/16 
 Pct Recovery = 100%  Analysis Date = 01/13/16 
 Pct Recovery = 100%  Analysis Date = 01/09/16 
 Pct Recovery = 100%  Analysis Date = 01/09/16 
 Pct Recovery = 100%  Analysis Date = 01/05/16 
 Pct Recovery = 100%  Analysis Date = 01/05/16 
 Pct Recovery = 100%  Analysis Date = 01/01/16 
 Pct Recovery = 100%  Analysis Date = 01/01/16 
 Pct Recovery = 100%  Analysis Date = 12/28/15 
 Pct Recovery = 100%  Analysis Date = 12/28/15 
 Pct Recovery = 100%  Analysis Date = 12/24/15 
 Pct Recovery = 100%  Analysis Date = 12/24/15 
 Pct Recovery = 100%  Analysis Date = 12/20/15 
 Pct Recovery = 99%  Analysis Date = 12/20/15 
 Pct Recovery = 99%  Analysis Date = 12/15/15 
 Pct Recovery = 99%  Analysis Date = 12/15/15 
 Pct Recovery = 99%  Analysis Date = 12/11/15 
 Pct Recovery = 99%  Analysis Date = 12/11/15 
 Pct Recovery = 99%  Analysis Date = 12/07/15 
 Pct Recovery = 99%  Analysis Date = 12/07/15 
 Pct Recovery = 99%  Analysis Date = 12/03/15 
 Pct Recovery = 99%  Analysis Date = 12/03/15 
 Pct Recovery = 99%  Analysis Date = 11/29/15 
 Pct Recovery = 99%  Analysis Date = 11/29/15 
 Pct Recovery = 99%  Analysis Date = 11/25/15 
 Pct Recovery = 99%  Analysis Date = 11/25/15 
 Pct Recovery = 99%  Analysis Date = 11/21/15 
 Pct Recovery = 99%  Analysis Date = 11/21/15 
 Pct Recovery = 99%  Analysis Date = 11/16/15 
 Pct Recovery = 99%  Analysis Date = 11/16/15 
 Pct Recovery = 99%  Analysis Date = 11/12/15 
 Pct Recovery = 99%  Analysis Date = 11/12/15 
 Pct Recovery = 99%  Analysis Date = 11/08/15 
 Pct Recovery = 99%  Analysis Date = 11/08/15 
 Pct Recovery = 99%  Analysis Date = 11/04/15 
 Pct Recovery = 99%  Analysis Date = 11/04/15 
 Pct Recovery = 99%  Analysis Date = 10/31/15 
 Pct Recovery = 99%  Analysis Date = 10/31/15 
 Pct Recovery = 99%  Analysis Date = 10/27/15 
 Pct Recovery = 99%  Analysis Date = 10/27/15 
 Pct Recovery = 99%  Analysis Date = 10/23/15 
 Pct Recovery = 99%  Analysis Date = 10/23/15 
 Pct Recovery = 99%  Analysis Date = 10/18/15 
 Pct Recovery = 99%  Analysis Date = 10/18/15 
 Pct Recovery = 99%  Analysis Date = 10/14/15 
 Pct Recovery = 99%  Analysis Date = 10/14/15 
 Pct Recovery = 99%  Analysis Date = 10/10/15 
 Pct Recovery = 99%  Analysis Date = 10/10/15 
 Pct Recovery = 99%  Analysis Date = 10/06/15 
 Pct Recovery = 99%  Analysis Date = 10/06/15 
 Pct Recovery = 99%  Analysis Date = 10/02/15 
 Pct Recovery = 99%  Analysis Date = 10/02/15 
 Pct Recovery = 99%  Analysis Date = 09/28/15 
 Pct Recovery = 99%  Analysis Date = 09/28/15 
 Pct Recovery = 99%  Analysis Date = 09/24/15 
 Pct Recovery = 99%  Analysis Date = 09/24/15 
 Pct Recovery = 99%  Analysis Date = 09/19/15 
 Pct Recovery = 99%  Analysis Date = 09/19/15 
 Pct Recovery = 99%  Analysis Date = 09/15/15 
 Pct Recovery = 99%  Analysis Date = 09/15/15 
 Pct Recovery = 99%  Analysis Date = 09/11/15 
 Pct Recovery = 100%  Analysis Date = 09/11/15 
 Pct Recovery = 100%  Analysis Date = 09/07/15 
 Pct Recovery = 100%  Analysis Date = 09/07/15 
 Pct Recovery = 100%  Analysis Date = 09/03/15 
 Pct Recovery = 100%  Analysis Date = 09/03/15 
 Pct Recovery = 100%  Analysis Date = 08/30/15 
 Pct Recovery = 100%  Analysis Date = 08/30/15 
 Pct Recovery = 100%  Analysis Date = 08/26/15 
 Pct Recovery = 100%  Analysis Date = 08/26/15 
 Pct Recovery = 100%  Analysis Date = 08/21/15 
 Pct Recovery = 100%  Analysis Date = 08/21/15 
 Pct Recovery = 100%  Analysis Date = 08/17/15 
 Pct Recovery = 100%  Analysis Date = 08/17/15 
 Pct Recovery = 100%  Analysis Date = 08/13/15 
 Pct Recovery = 100%  Analysis Date = 08/13/15 
 Pct Recovery = 100%  Analysis Date = 08/09/15 
 Pct Recovery = 100%  Analysis Date = 08/09/15 
 Pct Recovery = 100%  Analysis Date = 08/05/15 
 Pct Recovery = 100%  Analysis Date = 08/05/15 
 Pct Recovery = 100%  Analysis Date = 08/01/15 
 Pct Recovery = 100%  Analysis Date = 08/01/15 
 Pct Recovery = 100%  Analysis Date = 07/28/15 
 Pct Recovery = 101%  Analysis Date = 07/28/15 
 Pct Recovery = 101%  Analysis Date = 07/23/15 
 Pct Recovery = 101%  Analysis Date = 07/23/15 
 Pct Recovery = 101%  Analysis Date = 07/19/15 
 Pct Recovery = 101%  Analysis Date = 07/19/15 
 Pct Recovery = 101%  Analysis Date = 07/15/15 
 Pct Recovery = 101%  Analysis Date = 07/15/15 
 Pct Recovery = 101%  Analysis Date = 07/11/15 
 Pct Recovery = 101%  Analysis Date = 07/11/15 
 Pct Recovery = 101%  Analysis Date = 07/07/15 
 Pct Recovery = 101%  Analysis Date = 07/07/15 
 Pct Recovery = 101%  Analysis Date = 07/03/15 
 Pct Recovery = 101%  Analysis Date = 07/03/15 
 Pct Recovery = 101%  Analysis Date = 06/29/15 
 Pct Recovery = 101%  Analysis Date = 06/29/15 
 Pct Recovery = 101%  Analysis Date = 06/24/15 
 Pct Recovery = 101%  Analysis Date = 06/24/15 
 Pct Recovery = 101%  Analysis Date = 06/20/15 
 Pct Recovery = 101%  Analysis Date = 06/20/15 
 Pct Recovery = 101%  Analysis Date = 06/16/15 
 Pct Recovery = 101%  Analysis Date = 06/16/15 
 Pct Recovery = 101%  Analysis Date = 06/12/15 
 Pct Recovery = 102%  Analysis Date = 06/12/15 
 Pct Recovery = 102%  Analysis Date = 06/08/15 
 Pct Recovery = 102%  Analysis Date = 06/08/15 
 Pct Recovery = 102%  Analysis Date = 06/04/15 
 Pct Recovery = 102%  Analysis Date = 06/04/15 
 Pct Recovery = 102%  Analysis Date = 05/31/15 
 Pct Recovery = 102%  Analysis Date = 05/31/15 
 Pct Recovery = 102%  Analysis Date = 05/27/15 
 Pct Recovery = 102%  Analysis Date = 05/27/15 
 Pct Recovery = 102%  Analysis Date = 05/22/15 
 Pct Recovery = 102%  Analysis Date = 05/22/15 
 Pct Recovery = 102%  Analysis Date = 05/18/15 
 Pct Recovery = 102%  Analysis Date = 05/18/15 
 Pct Recovery = 102%  Analysis Date = 05/14/15 
 Pct Recovery = 102%  Analysis Date = 05/14/15 
 Pct Recovery = 102%  Analysis Date = 05/10/15 
 Pct Recovery = 102%  Analysis Date = 05/10/15 
 Pct Recovery = 102%  Analysis Date = 05/06/15 
 Pct Recovery = 102%  Analysis Date = 05/06/15 
 Pct Recovery = 102%  Analysis Date = 05/02/15 
 Pct Recovery = 102%  Analysis Date = 05/02/15 
 Pct Recovery = 102%  Analysis Date = 04/28/15 
 Pct Recovery = 102%  Analysis Date = 04/28/15 
 Pct Recovery = 102%  Analysis Date = 04/23/15 
 Pct Recovery = 102%  Analysis Date = 04/23/15 
 Pct Recovery = 102%  Analysis Date = 04/19/15 
 Pct Recovery = 102%  Analysis Date = 04/19/15 
 Pct Recovery = 102%  Analysis Date = 04/15/15 
 Pct Recovery = 102%  Analysis Date = 04/15/15 
 Pct Recovery = 102%  Analysis Date = 04/11/15 
 Pct Recovery = 102%  Analysis Date = 04/11/15 
 Pct Recovery = 102%  Analysis Date = 04/07/15 
 Pct Recovery = 102%  Analysis Date = 04/07/15 
 Pct Recovery = 102%  Analysis Date = 04/03/15 
 Pct Recovery = 102%  Analysis Date = 04/03/15 
 Pct Recovery = 102%  Analysis Date = 03/30/15 
 Pct Recovery = 102%  Analysis Date = 03/30/15 
 Pct Recovery = 102%  Analysis Date = 03/25/15 
 Pct Recovery = 102%  Analysis Date = 03/25/15 
 Pct Recovery = 102%  Analysis Date = 03/21/15 
 Pct Recovery = 102%  Analysis Date = 03/21/15 
 Pct Recovery = 102%  Analysis Date = 03/17/15 
 Pct Recovery = 102%  Analysis Date = 03/17/15 
 Pct Recovery = 102%  Analysis Date = 03/13/15 
 Pct Recovery = 102%  Analysis Date = 03/13/15 
 Pct Recovery = 102%  Analysis Date = 03/09/15 
 Pct Recovery = 102%  Analysis Date = 03/09/15 
 Pct Recovery = 102%  Analysis Date = 03/05/15 
 Pct Recovery = 103%  Analysis Date = 03/05/15 
 Pct Recovery = 103%  Analysis Date = 03/01/15 
 Pct Recovery = 103%  Analysis Date = 03/01/15 
 Pct Recovery = 103%  Analysis Date = 02/24/15 
 Pct Recovery = 103%  Analysis Date = 02/24/15 
 Pct Recovery = 103%  Analysis Date = 02/20/15 
 Pct Recovery = 103%  Analysis Date = 02/20/15 
 Pct Recovery = 103%  Analysis Date = 02/16/15 
 Pct Recovery = 103%  Analysis Date = 02/16/15 
 Pct Recovery = 103%  Analysis Date = 02/12/15 
 Pct Recovery = 103%  Analysis Date = 02/12/15 
 Pct Recovery = 103%  Analysis Date = 02/08/15 
 Pct Recovery = 103%  Analysis Date = 02/08/15 
 Pct Recovery = 103%  Analysis Date = 02/04/15 
 Pct Recovery = 103%  Analysis Date = 02/04/15 
 Pct Recovery = 103%  Analysis Date = 01/31/15 
 Pct Recovery = 103%  Analysis Date = 01/31/15 
 Pct Recovery = 103%  Analysis Date = 01/26/15 
 Pct Recovery = 103%  Analysis Date = 01/26/15 
 Pct Recovery = 103%  Analysis Date = 01/22/15 
 Pct Recovery = 103%  Analysis Date = 01/22/15 
 Pct Recovery = 103%  Analysis Date = 01/18/15 
 Pct Recovery = 103%  Analysis Date = 01/18/15 
 Pct Recovery = 103%  Analysis Date = 01/14/15 
 Pct Recovery = 103%  Analysis Date = 01/14/15 
 Pct Recovery = 103%  Analysis Date = 01/10/15 
 Pct Recovery = 103%  Analysis Date = 01/10/15 
 Pct Recovery = 103%  Analysis Date = 01/06/15 
 Pct Recovery = 103%  Analysis Date = 01/06/15 
 Pct Recovery = 103%  Analysis Date = 01/02/15 
 Pct Recovery = 103%  Analysis Date = 01/02/15 
 Pct Recovery = 103%  Analysis Date = 12/28/14 
 Pct Recovery = 103%  Analysis Date = 12/28/14 
 Pct Recovery = 103%  Analysis Date = 12/24/14 
 Pct Recovery = 103%  Analysis Date = 12/24/14 
 Pct Recovery = 103%  Analysis Date = 12/20/14 
 Pct Recovery = 103%  Analysis Date = 12/20/14 
 Pct Recovery = 103%  Analysis Date = 12/16/14 
 Pct Recovery = 103%  Analysis Date = 12/16/14 
 Pct Recovery = 103%  Analysis Date = 12/12/14 
 Pct Recovery = 103%  Analysis Date = 12/12/14 
 Pct Recovery = 103%  Analysis Date = 12/08/14 
 Pct Recovery = 103%  Analysis Date = 12/08/14 
 Pct Recovery = 103%  Analysis Date = 12/04/14 
 Pct Recovery = 103%  Analysis Date = 12/04/14 
 Pct Recovery = 103%  Analysis Date = 11/29/14 
 Pct Recovery = 103%  Analysis Date = 11/29/14 
 Pct Recovery = 103%  Analysis Date = 11/25/14 
 Pct Recovery = 103%  Analysis Date = 11/25/14 
 Pct Recovery = 103%  Analysis Date = 11/21/14 
 Pct Recovery = 103%  Analysis Date = 11/21/14 
 Pct Recovery = 103%  Analysis Date = 11/17/14 
 Pct Recovery = 103%  Analysis Date = 11/17/14 
 Pct Recovery = 103%  Analysis Date = 11/13/14 
 Pct Recovery = 103%  Analysis Date = 11/13/14 
 Pct Recovery = 103%  Analysis Date = 11/09/14 
 Pct Recovery = 103%  Analysis Date = 11/09/14 
 Pct Recovery = 103%  Analysis Date = 11/05/14 
 Pct Recovery = 103%  Analysis Date = 11/05/14 
 Pct Recovery = 103%  Analysis Date = 11/01/14 
 Pct Recovery = 103%  Analysis Date = 11/01/14 
 Pct Recovery = 103%  Analysis Date = 10/27/14 
 Pct Recovery = 103%  Analysis Date = 10/27/14 
 Pct Recovery = 103%  Analysis Date = 10/23/14 
 Pct Recovery = 103%  Analysis Date = 10/23/14 
 Pct Recovery = 103%  Analysis Date = 10/19/14 
 Pct Recovery = 103%  Analysis Date = 10/19/14 
 Pct Recovery = 103%  Analysis Date = 10/15/14 
 Pct Recovery = 103%  Analysis Date = 10/15/14 
 Pct Recovery = 103%  Analysis Date = 10/11/14 
 Pct Recovery = 103%  Analysis Date = 10/11/14 
 Pct Recovery = 103%  Analysis Date = 10/07/14 
 Pct Recovery = 103%  Analysis Date = 10/07/14 
 Pct Recovery = 103%  Analysis Date = 10/03/14 
 Pct Recovery = 103%  Analysis Date = 10/03/14 
 Pct Recovery = 103%  Analysis Date = 09/28/14 
 Pct Recovery = 103%  Analysis Date = 09/28/14 
 Pct Recovery = 103%  Analysis Date = 09/24/14 
 Pct Recovery = 103%  Analysis Date = 09/24/14 
 Pct Recovery = 103%  Analysis Date = 09/20/14 
 Pct Recovery = 103%  Analysis Date = 09/20/14 
 Pct Recovery = 103%  Analysis Date = 09/16/14 
 Pct Recovery = 103%  Analysis Date = 09/16/14 
 Pct Recovery = 103%  Analysis Date = 09/12/14 
 Pct Recovery = 103%  Analysis Date = 09/12/14 
 Pct Recovery = 103%  Analysis Date = 09/08/14 
 Pct Recovery = 103%  Analysis Date = 09/08/14 
 Pct Recovery = 103%  Analysis Date = 09/04/14 
 Pct Recovery = 103%  Analysis Date = 09/04/14 
 Pct Recovery = 103%  Analysis Date = 08/30/14 
 Pct Recovery = 103%  Analysis Date = 08/30/14 
 Pct Recovery = 103%  Analysis Date = 08/26/14 
 Pct Recovery = 103%  Analysis Date = 08/26/14 
 Pct Recovery = 103%  Analysis Date = 08/22/14 
 Pct Recovery = 103%  Analysis Date = 08/22/14 
 Pct Recovery = 103%  Analysis Date = 08/18/14 
 Pct Recovery = 103%  Analysis Date = 08/18/14 
 Pct Recovery = 103%  Analysis Date = 08/14/14 
 Pct Recovery = 103%  Analysis Date = 08/14/14 
 Pct Recovery = 103%  Analysis Date = 08/10/14 
 Pct Recovery = 103%  Analysis Date = 08/10/14 
 Pct Recovery = 103%  Analysis Date = 08/06/14 
 Pct Recovery = 103%  Analysis Date = 08/06/14 
 Pct Recovery = 103%  Analysis Date = 08/01/14 
 Pct Recovery = 103%  Analysis Date = 08/01/14 
 Pct Recovery = 103%  Analysis Date = 07/28/14 
 Pct Recovery = 103%  Analysis Date = 07/28/14 
 Pct Recovery = 103%  Analysis Date = 07/24/14 
 Pct Recovery = 103%  Analysis Date = 07/24/14 
 Pct Recovery = 103%  Analysis Date = 07/20/14 
 Pct Recovery = 103%  Analysis Date = 07/20/14 
 Pct Recovery = 103%  Analysis Date = 07/16/14 
 Pct Recovery = 103%  Analysis Date = 07/16/14 
 Pct Recovery = 103%  Analysis Date = 07/12/14 
 Pct Recovery = 103%  Analysis Date = 07/12/14 
 Pct Recovery = 103%  Analysis Date = 07/08/14 
 Pct Recovery = 103%  Analysis Date = 07/08/14 
 Pct Recovery = 103%  Analysis Date = 07/03/14 
 Pct Recovery = 103%  Analysis Date = 07/03/14 
 Pct Recovery = 103%  Analysis Date = 06/29/14 
 Pct Recovery = 103%  Analysis Date = 06/29/14 
 Pct Recovery = 103%  Analysis Date = 06/25/14 
 Pct Recovery = 103%  Analysis Date = 06/25/14 
 Pct Recovery = 103%  Analysis Date = 06/21/14 
 Pct Recovery = 103%  Analysis Date = 06/21/14 
 Pct Recovery = 103%  Analysis Date = 06/17/14 
 Pct Recovery = 103%  Analysis Date = 06/17/14 
 Pct Recovery = 103%  Analysis Date = 06/13/14 
 Pct Recovery = 104%  Analysis Date = 06/13/14 
 Pct Recovery = 104%  Analysis Date = 06/09/14 
 Pct Recovery = 104%  Analysis Date = 06/09/14 
 Pct Recovery = 104%  Analysis Date = 06/04/14 
 Pct Recovery = 104%  Analysis Date = 06/04/14 
 Pct Recovery = 104%  Analysis Date = 05/31/14 
 Pct Recovery = 104%  Analysis Date = 05/31/14 
 Pct Recovery = 104%  Analysis Date = 05/27/14 
 Pct Recovery = 104%  Analysis Date = 05/27/14 
 Pct Recovery = 104%  Analysis Date = 05/23/14 
 Pct Recovery = 104%  Analysis Date = 05/23/14 
 Pct Recovery = 104%  Analysis Date = 05/19/14 
 Pct Recovery = 104%  Analysis Date = 05/19/14 
 Pct Recovery = 104%  Analysis Date = 05/15/14 
 Pct Recovery = 104%  Analysis Date = 05/15/14 
 Pct Recovery = 104%  Analysis Date = 05/11/14 
 Pct Recovery = 104%  Analysis Date = 05/11/14 
 Pct Recovery = 104%  Analysis Date = 05/07/14 
 Pct Recovery = 104%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
1,2-DICHLOROPROPANE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 38 102% 8% 102% 9%
Total 38 102% 8% 102% 9%

Sample Statistics
1,2-DICHLOROPROPANE

Characteristic N % % Basis
Plotted 38 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 38 .  
False Negatives 0 0% 0 out of 38
Not Spiked 17 .  
False Positives 0 0% 0 out of 17

BQS OBSP Determination:
1,3-DIOXOLANE
METHOD: 4437 , TESTIDCODE: 81583GM016
Open Data Set

 Analysis Date = 07/06/16 
 SpikeMix = Accu 216041354: 40 µl & NSI 041516: 40 µl & NSI 041416HVOC: 40 µl 
 Pct Recovery = 117%  Analysis Date = 07/29/16 
 SpikeMix = Supelco LC20145V: 40 µl & NSI 041516: 40 µl & NSI 041416HVOC: 40 µl 
 Pct Recovery = 107%  Analysis Date = 08/11/16 
 SpikeMix = Phenova B20160303: 25 µl & Supelco LC20145V: 25 µl & NSI 041416HVOC: 25 µl 
 Pct Recovery = 94%  Analysis Date = 05/21/16 
 SpikeMix = Supelco LC20145V: 25 µl & NSI 041516: 25 µl & NSI 041416HVOC: 25 µl 
 Pct Recovery = 156%  Analysis Date = 03/19/15 
 SpikeMix = Supelco LC06437: 20 µl & NSI 031814: 20 µl 
 Pct Recovery = 159%  Analysis Date = 01/10/15 
 SpikeMix = Abs 032014: 20 µl & ERA 0321-14-05A: 20 µl 
 Pct Recovery = 100%  Analysis Date = 07/23/14 
 SpikeMix = Accu 214031128: 20 µl & Abs 032014: 20 µl 
 Pct Recovery = 122%  Analysis Date = 07/03/14 
 SpikeMix = Abs 032014: 20 µl & ChemService 2615700: 20 µl 
 Pct Recovery = 105%  Analysis Date = 06/06/14 
 SpikeMix = NSI 031814: 20 µl & ChemService 2615700: 20 µl 
 Pct Recovery = 93%  Analysis Date = 05/07/14 
 SpikeMix = NSI 031814: 20 µl & Accu 214031128: 20 µl 
 Pct Recovery = 105%  Analysis Date = 01/22/16 
 SpikeMix = NSI 050515HVOC: 25 µl & ERA 0601-15-05: 25 µl 
 Pct Recovery = 99%  Analysis Date = 10/09/15 
 SpikeMix = ERA 0601-15-05: 25 µl & Accu 215041338: 25 µl 
 Pct Recovery = 87%  Analysis Date = 06/26/15 
 SpikeMix = ChemService 3818700: 25 µl & Accu 215041338: 25 µl 
 Pct Recovery = 93%  Analysis Date = 06/25/15 
 SpikeMix = ChemService 3818700: 25 µl & NSI 050515HVOC: 25 µl 
 Pct Recovery = 108%  Analysis Date = 08/12/16 
 SpikeMix = Accu 216041354: 15 µl & Abs 060916HVOC: 15 µl 
 Pct Recovery = 97%  Analysis Date = 07/06/16 
 SpikeMix = Phenova B20160303: 15 µl & Accu 216041354: 15 µl & NSI 041416HVOC: 15 µl 
 Pct Recovery = 92%  Analysis Date = 06/23/16 
 SpikeMix = . 
 Pct Recovery = 78%  Analysis Date = 05/20/16 
 SpikeMix = Accu 216041354: 15 µl & NSI 041516: 15 µl & Accu 216041225: 15 µl 
 Pct Recovery = 136%  Analysis Date = 07/27/16 
 SpikeMix = ChemService 5082800: 15 µl & Supelco LC20145V: 15 µl & Accu 216041225: 15 µl 
 Pct Recovery = 91%  Analysis Date = 04/28/16 
 SpikeMix = ChemService 3818700: 15 µl & Supelco LC13544: 15 µl 
 Pct Recovery = 105%  Analysis Date = 09/24/15 
 SpikeMix = Abs 040315: 15 µl & ERA 0601-15-05: 15 µl 
 Pct Recovery = 101%  Analysis Date = 08/24/15 
 SpikeMix = ERA 0601-15-05: 15 µl & Supelco LC13544: 15 µl 
 Pct Recovery = 83%  Analysis Date = 06/16/15 
 SpikeMix = ChemService 3818700: 15 µl & NSI 050515HVOC: 15 µl 
 Pct Recovery = 100%  Analysis Date = 05/14/15 
 SpikeMix = ChemService 3818700: 15 µl & Supelco LC13544: 15 µl 
 Pct Recovery = 110%  Analysis Date = 04/25/15 
 SpikeMix = Abs 032014: 10 µl & ERA 0321-14-05A: 10 µl 
 Pct Recovery = 105%  Analysis Date = 12/13/14 
 SpikeMix = Accu 214031128: 10 µl & NSI 031814: 10 µl 
 Pct Recovery = 104%  Analysis Date = 09/11/14 
 SpikeMix = Accu 214031128: 10 µl & Abs 032014: 10 µl 
 Pct Recovery = 122%  Analysis Date = 07/30/14 
 SpikeMix = NSI 031814: 10 µl & ChemService 2615700: 10 µl 
 Pct Recovery = 98%  Analysis Date = 06/17/14 
 SpikeMix = Supelco LC06437: 10 µl & Abs 032014: 10 µl 
 Pct Recovery = 118%  Analysis Date = 04/09/16 
 SpikeMix = Abs 040315: 10 µl & ChemService 3818700: 10 µl 
 Pct Recovery = 118%  Analysis Date = 02/12/16 
 SpikeMix = ERA 0601-15-05: 10 µl & Accu 215041338: 10 µl 
 Pct Recovery = 97%  Analysis Date = 12/10/15 
 SpikeMix = ChemService 3818700: 10 µl & Supelco LC13544: 10 µl 
 Pct Recovery = 97%  Analysis Date = 12/05/15 
 SpikeMix = NSI 050515HVOC: 10 µl & ERA 0601-15-05: 10 µl 
 Pct Recovery = 95%  Analysis Date = 11/14/15 
 SpikeMix = ERA 0601-15-05: 10 µl 
 Pct Recovery = 97%  Analysis Date = 10/23/15 
 SpikeMix = Abs 040315: 10 µl & ChemService 3818700: 10 µl 
 Pct Recovery = 126%  Analysis Date = 08/14/15 
 SpikeMix = Abs 040315: 10 µl & ERA 0601-15-05: 10 µl 
 Pct Recovery = 87%  Analysis Date = 05/20/15 
 SpikeMix = ChemService 3818700: 10 µl & Accu 215041338: 10 µl 
 Pct Recovery = 126%  Analysis Date = 08/11/16 
 Pct Recovery = 105%  Analysis Date = 08/07/16 
 Pct Recovery = 105%  Analysis Date = 08/07/16 
 Pct Recovery = 105%  Analysis Date = 08/03/16 
 Pct Recovery = 105%  Analysis Date = 08/03/16 
 Pct Recovery = 105%  Analysis Date = 07/30/16 
 Pct Recovery = 105%  Analysis Date = 07/30/16 
 Pct Recovery = 105%  Analysis Date = 07/26/16 
 Pct Recovery = 106%  Analysis Date = 07/26/16 
 Pct Recovery = 106%  Analysis Date = 07/22/16 
 Pct Recovery = 106%  Analysis Date = 07/22/16 
 Pct Recovery = 106%  Analysis Date = 07/18/16 
 Pct Recovery = 106%  Analysis Date = 07/18/16 
 Pct Recovery = 106%  Analysis Date = 07/14/16 
 Pct Recovery = 106%  Analysis Date = 07/14/16 
 Pct Recovery = 106%  Analysis Date = 07/09/16 
 Pct Recovery = 106%  Analysis Date = 07/09/16 
 Pct Recovery = 106%  Analysis Date = 07/05/16 
 Pct Recovery = 106%  Analysis Date = 07/05/16 
 Pct Recovery = 106%  Analysis Date = 07/01/16 
 Pct Recovery = 106%  Analysis Date = 07/01/16 
 Pct Recovery = 106%  Analysis Date = 06/27/16 
 Pct Recovery = 106%  Analysis Date = 06/27/16 
 Pct Recovery = 106%  Analysis Date = 06/23/16 
 Pct Recovery = 106%  Analysis Date = 06/23/16 
 Pct Recovery = 106%  Analysis Date = 06/19/16 
 Pct Recovery = 106%  Analysis Date = 06/19/16 
 Pct Recovery = 106%  Analysis Date = 06/15/16 
 Pct Recovery = 106%  Analysis Date = 06/15/16 
 Pct Recovery = 106%  Analysis Date = 06/10/16 
 Pct Recovery = 106%  Analysis Date = 06/10/16 
 Pct Recovery = 106%  Analysis Date = 06/06/16 
 Pct Recovery = 106%  Analysis Date = 06/06/16 
 Pct Recovery = 106%  Analysis Date = 06/02/16 
 Pct Recovery = 106%  Analysis Date = 06/02/16 
 Pct Recovery = 106%  Analysis Date = 05/29/16 
 Pct Recovery = 106%  Analysis Date = 05/29/16 
 Pct Recovery = 106%  Analysis Date = 05/25/16 
 Pct Recovery = 106%  Analysis Date = 05/25/16 
 Pct Recovery = 106%  Analysis Date = 05/21/16 
 Pct Recovery = 106%  Analysis Date = 05/21/16 
 Pct Recovery = 106%  Analysis Date = 05/17/16 
 Pct Recovery = 106%  Analysis Date = 05/17/16 
 Pct Recovery = 106%  Analysis Date = 05/12/16 
 Pct Recovery = 106%  Analysis Date = 05/12/16 
 Pct Recovery = 106%  Analysis Date = 05/08/16 
 Pct Recovery = 106%  Analysis Date = 05/08/16 
 Pct Recovery = 106%  Analysis Date = 05/04/16 
 Pct Recovery = 106%  Analysis Date = 05/04/16 
 Pct Recovery = 106%  Analysis Date = 04/30/16 
 Pct Recovery = 106%  Analysis Date = 04/30/16 
 Pct Recovery = 106%  Analysis Date = 04/26/16 
 Pct Recovery = 105%  Analysis Date = 04/26/16 
 Pct Recovery = 105%  Analysis Date = 04/22/16 
 Pct Recovery = 105%  Analysis Date = 04/22/16 
 Pct Recovery = 105%  Analysis Date = 04/18/16 
 Pct Recovery = 105%  Analysis Date = 04/18/16 
 Pct Recovery = 105%  Analysis Date = 04/13/16 
 Pct Recovery = 105%  Analysis Date = 04/13/16 
 Pct Recovery = 105%  Analysis Date = 04/09/16 
 Pct Recovery = 105%  Analysis Date = 04/09/16 
 Pct Recovery = 105%  Analysis Date = 04/05/16 
 Pct Recovery = 105%  Analysis Date = 04/05/16 
 Pct Recovery = 105%  Analysis Date = 04/01/16 
 Pct Recovery = 105%  Analysis Date = 04/01/16 
 Pct Recovery = 105%  Analysis Date = 03/28/16 
 Pct Recovery = 105%  Analysis Date = 03/28/16 
 Pct Recovery = 105%  Analysis Date = 03/24/16 
 Pct Recovery = 105%  Analysis Date = 03/24/16 
 Pct Recovery = 105%  Analysis Date = 03/20/16 
 Pct Recovery = 104%  Analysis Date = 03/20/16 
 Pct Recovery = 104%  Analysis Date = 03/15/16 
 Pct Recovery = 104%  Analysis Date = 03/15/16 
 Pct Recovery = 104%  Analysis Date = 03/11/16 
 Pct Recovery = 104%  Analysis Date = 03/11/16 
 Pct Recovery = 104%  Analysis Date = 03/07/16 
 Pct Recovery = 104%  Analysis Date = 03/07/16 
 Pct Recovery = 104%  Analysis Date = 03/03/16 
 Pct Recovery = 104%  Analysis Date = 03/03/16 
 Pct Recovery = 104%  Analysis Date = 02/28/16 
 Pct Recovery = 104%  Analysis Date = 02/28/16 
 Pct Recovery = 104%  Analysis Date = 02/24/16 
 Pct Recovery = 104%  Analysis Date = 02/24/16 
 Pct Recovery = 104%  Analysis Date = 02/20/16 
 Pct Recovery = 104%  Analysis Date = 02/20/16 
 Pct Recovery = 104%  Analysis Date = 02/15/16 
 Pct Recovery = 103%  Analysis Date = 02/15/16 
 Pct Recovery = 103%  Analysis Date = 02/11/16 
 Pct Recovery = 103%  Analysis Date = 02/11/16 
 Pct Recovery = 103%  Analysis Date = 02/07/16 
 Pct Recovery = 103%  Analysis Date = 02/07/16 
 Pct Recovery = 103%  Analysis Date = 02/03/16 
 Pct Recovery = 103%  Analysis Date = 02/03/16 
 Pct Recovery = 103%  Analysis Date = 01/30/16 
 Pct Recovery = 103%  Analysis Date = 01/30/16 
 Pct Recovery = 103%  Analysis Date = 01/26/16 
 Pct Recovery = 103%  Analysis Date = 01/26/16 
 Pct Recovery = 103%  Analysis Date = 01/22/16 
 Pct Recovery = 103%  Analysis Date = 01/22/16 
 Pct Recovery = 103%  Analysis Date = 01/17/16 
 Pct Recovery = 103%  Analysis Date = 01/17/16 
 Pct Recovery = 103%  Analysis Date = 01/13/16 
 Pct Recovery = 103%  Analysis Date = 01/13/16 
 Pct Recovery = 103%  Analysis Date = 01/09/16 
 Pct Recovery = 102%  Analysis Date = 01/09/16 
 Pct Recovery = 102%  Analysis Date = 01/05/16 
 Pct Recovery = 102%  Analysis Date = 01/05/16 
 Pct Recovery = 102%  Analysis Date = 01/01/16 
 Pct Recovery = 102%  Analysis Date = 01/01/16 
 Pct Recovery = 102%  Analysis Date = 12/28/15 
 Pct Recovery = 102%  Analysis Date = 12/28/15 
 Pct Recovery = 102%  Analysis Date = 12/24/15 
 Pct Recovery = 102%  Analysis Date = 12/24/15 
 Pct Recovery = 102%  Analysis Date = 12/20/15 
 Pct Recovery = 102%  Analysis Date = 12/20/15 
 Pct Recovery = 102%  Analysis Date = 12/15/15 
 Pct Recovery = 102%  Analysis Date = 12/15/15 
 Pct Recovery = 102%  Analysis Date = 12/11/15 
 Pct Recovery = 102%  Analysis Date = 12/11/15 
 Pct Recovery = 102%  Analysis Date = 12/07/15 
 Pct Recovery = 101%  Analysis Date = 12/07/15 
 Pct Recovery = 101%  Analysis Date = 12/03/15 
 Pct Recovery = 101%  Analysis Date = 12/03/15 
 Pct Recovery = 101%  Analysis Date = 11/29/15 
 Pct Recovery = 101%  Analysis Date = 11/29/15 
 Pct Recovery = 101%  Analysis Date = 11/25/15 
 Pct Recovery = 101%  Analysis Date = 11/25/15 
 Pct Recovery = 101%  Analysis Date = 11/21/15 
 Pct Recovery = 101%  Analysis Date = 11/21/15 
 Pct Recovery = 101%  Analysis Date = 11/16/15 
 Pct Recovery = 101%  Analysis Date = 11/16/15 
 Pct Recovery = 101%  Analysis Date = 11/12/15 
 Pct Recovery = 101%  Analysis Date = 11/12/15 
 Pct Recovery = 101%  Analysis Date = 11/08/15 
 Pct Recovery = 101%  Analysis Date = 11/08/15 
 Pct Recovery = 101%  Analysis Date = 11/04/15 
 Pct Recovery = 101%  Analysis Date = 11/04/15 
 Pct Recovery = 101%  Analysis Date = 10/31/15 
 Pct Recovery = 101%  Analysis Date = 10/31/15 
 Pct Recovery = 101%  Analysis Date = 10/27/15 
 Pct Recovery = 101%  Analysis Date = 10/27/15 
 Pct Recovery = 101%  Analysis Date = 10/23/15 
 Pct Recovery = 101%  Analysis Date = 10/23/15 
 Pct Recovery = 101%  Analysis Date = 10/18/15 
 Pct Recovery = 101%  Analysis Date = 10/18/15 
 Pct Recovery = 101%  Analysis Date = 10/14/15 
 Pct Recovery = 101%  Analysis Date = 10/14/15 
 Pct Recovery = 101%  Analysis Date = 10/10/15 
 Pct Recovery = 101%  Analysis Date = 10/10/15 
 Pct Recovery = 101%  Analysis Date = 10/06/15 
 Pct Recovery = 101%  Analysis Date = 10/06/15 
 Pct Recovery = 101%  Analysis Date = 10/02/15 
 Pct Recovery = 101%  Analysis Date = 10/02/15 
 Pct Recovery = 101%  Analysis Date = 09/28/15 
 Pct Recovery = 101%  Analysis Date = 09/28/15 
 Pct Recovery = 101%  Analysis Date = 09/24/15 
 Pct Recovery = 101%  Analysis Date = 09/24/15 
 Pct Recovery = 101%  Analysis Date = 09/19/15 
 Pct Recovery = 101%  Analysis Date = 09/19/15 
 Pct Recovery = 101%  Analysis Date = 09/15/15 
 Pct Recovery = 101%  Analysis Date = 09/15/15 
 Pct Recovery = 101%  Analysis Date = 09/11/15 
 Pct Recovery = 101%  Analysis Date = 09/11/15 
 Pct Recovery = 101%  Analysis Date = 09/07/15 
 Pct Recovery = 102%  Analysis Date = 09/07/15 
 Pct Recovery = 102%  Analysis Date = 09/03/15 
 Pct Recovery = 102%  Analysis Date = 09/03/15 
 Pct Recovery = 102%  Analysis Date = 08/30/15 
 Pct Recovery = 102%  Analysis Date = 08/30/15 
 Pct Recovery = 102%  Analysis Date = 08/26/15 
 Pct Recovery = 103%  Analysis Date = 08/26/15 
 Pct Recovery = 103%  Analysis Date = 08/21/15 
 Pct Recovery = 103%  Analysis Date = 08/21/15 
 Pct Recovery = 103%  Analysis Date = 08/17/15 
 Pct Recovery = 103%  Analysis Date = 08/17/15 
 Pct Recovery = 103%  Analysis Date = 08/13/15 
 Pct Recovery = 103%  Analysis Date = 08/13/15 
 Pct Recovery = 103%  Analysis Date = 08/09/15 
 Pct Recovery = 104%  Analysis Date = 08/09/15 
 Pct Recovery = 104%  Analysis Date = 08/05/15 
 Pct Recovery = 104%  Analysis Date = 08/05/15 
 Pct Recovery = 104%  Analysis Date = 08/01/15 
 Pct Recovery = 104%  Analysis Date = 08/01/15 
 Pct Recovery = 104%  Analysis Date = 07/28/15 
 Pct Recovery = 104%  Analysis Date = 07/28/15 
 Pct Recovery = 104%  Analysis Date = 07/23/15 
 Pct Recovery = 105%  Analysis Date = 07/23/15 
 Pct Recovery = 105%  Analysis Date = 07/19/15 
 Pct Recovery = 105%  Analysis Date = 07/19/15 
 Pct Recovery = 105%  Analysis Date = 07/15/15 
 Pct Recovery = 105%  Analysis Date = 07/15/15 
 Pct Recovery = 105%  Analysis Date = 07/11/15 
 Pct Recovery = 105%  Analysis Date = 07/11/15 
 Pct Recovery = 105%  Analysis Date = 07/07/15 
 Pct Recovery = 106%  Analysis Date = 07/07/15 
 Pct Recovery = 106%  Analysis Date = 07/03/15 
 Pct Recovery = 106%  Analysis Date = 07/03/15 
 Pct Recovery = 106%  Analysis Date = 06/29/15 
 Pct Recovery = 106%  Analysis Date = 06/29/15 
 Pct Recovery = 106%  Analysis Date = 06/24/15 
 Pct Recovery = 107%  Analysis Date = 06/24/15 
 Pct Recovery = 107%  Analysis Date = 06/20/15 
 Pct Recovery = 107%  Analysis Date = 06/20/15 
 Pct Recovery = 107%  Analysis Date = 06/16/15 
 Pct Recovery = 107%  Analysis Date = 06/16/15 
 Pct Recovery = 107%  Analysis Date = 06/12/15 
 Pct Recovery = 107%  Analysis Date = 06/12/15 
 Pct Recovery = 107%  Analysis Date = 06/08/15 
 Pct Recovery = 107%  Analysis Date = 06/08/15 
 Pct Recovery = 107%  Analysis Date = 06/04/15 
 Pct Recovery = 108%  Analysis Date = 06/04/15 
 Pct Recovery = 108%  Analysis Date = 05/31/15 
 Pct Recovery = 108%  Analysis Date = 05/31/15 
 Pct Recovery = 108%  Analysis Date = 05/27/15 
 Pct Recovery = 108%  Analysis Date = 05/27/15 
 Pct Recovery = 108%  Analysis Date = 05/22/15 
 Pct Recovery = 108%  Analysis Date = 05/22/15 
 Pct Recovery = 108%  Analysis Date = 05/18/15 
 Pct Recovery = 109%  Analysis Date = 05/18/15 
 Pct Recovery = 109%  Analysis Date = 05/14/15 
 Pct Recovery = 109%  Analysis Date = 05/14/15 
 Pct Recovery = 109%  Analysis Date = 05/10/15 
 Pct Recovery = 109%  Analysis Date = 05/10/15 
 Pct Recovery = 109%  Analysis Date = 05/06/15 
 Pct Recovery = 109%  Analysis Date = 05/06/15 
 Pct Recovery = 109%  Analysis Date = 05/02/15 
 Pct Recovery = 109%  Analysis Date = 05/02/15 
 Pct Recovery = 109%  Analysis Date = 04/28/15 
 Pct Recovery = 110%  Analysis Date = 04/28/15 
 Pct Recovery = 110%  Analysis Date = 04/23/15 
 Pct Recovery = 110%  Analysis Date = 04/23/15 
 Pct Recovery = 110%  Analysis Date = 04/19/15 
 Pct Recovery = 110%  Analysis Date = 04/19/15 
 Pct Recovery = 110%  Analysis Date = 04/15/15 
 Pct Recovery = 110%  Analysis Date = 04/15/15 
 Pct Recovery = 110%  Analysis Date = 04/11/15 
 Pct Recovery = 111%  Analysis Date = 04/11/15 
 Pct Recovery = 111%  Analysis Date = 04/07/15 
 Pct Recovery = 111%  Analysis Date = 04/07/15 
 Pct Recovery = 111%  Analysis Date = 04/03/15 
 Pct Recovery = 111%  Analysis Date = 04/03/15 
 Pct Recovery = 111%  Analysis Date = 03/30/15 
 Pct Recovery = 111%  Analysis Date = 03/30/15 
 Pct Recovery = 111%  Analysis Date = 03/25/15 
 Pct Recovery = 111%  Analysis Date = 03/25/15 
 Pct Recovery = 111%  Analysis Date = 03/21/15 
 Pct Recovery = 112%  Analysis Date = 03/21/15 
 Pct Recovery = 112%  Analysis Date = 03/17/15 
 Pct Recovery = 112%  Analysis Date = 03/17/15 
 Pct Recovery = 112%  Analysis Date = 03/13/15 
 Pct Recovery = 112%  Analysis Date = 03/13/15 
 Pct Recovery = 112%  Analysis Date = 03/09/15 
 Pct Recovery = 112%  Analysis Date = 03/09/15 
 Pct Recovery = 112%  Analysis Date = 03/05/15 
 Pct Recovery = 112%  Analysis Date = 03/05/15 
 Pct Recovery = 112%  Analysis Date = 03/01/15 
 Pct Recovery = 112%  Analysis Date = 03/01/15 
 Pct Recovery = 112%  Analysis Date = 02/24/15 
 Pct Recovery = 112%  Analysis Date = 02/24/15 
 Pct Recovery = 112%  Analysis Date = 02/20/15 
 Pct Recovery = 112%  Analysis Date = 02/20/15 
 Pct Recovery = 112%  Analysis Date = 02/16/15 
 Pct Recovery = 112%  Analysis Date = 02/16/15 
 Pct Recovery = 112%  Analysis Date = 02/12/15 
 Pct Recovery = 111%  Analysis Date = 02/12/15 
 Pct Recovery = 111%  Analysis Date = 02/08/15 
 Pct Recovery = 111%  Analysis Date = 02/08/15 
 Pct Recovery = 111%  Analysis Date = 02/04/15 
 Pct Recovery = 111%  Analysis Date = 02/04/15 
 Pct Recovery = 111%  Analysis Date = 01/31/15 
 Pct Recovery = 111%  Analysis Date = 01/31/15 
 Pct Recovery = 111%  Analysis Date = 01/26/15 
 Pct Recovery = 111%  Analysis Date = 01/26/15 
 Pct Recovery = 111%  Analysis Date = 01/22/15 
 Pct Recovery = 111%  Analysis Date = 01/22/15 
 Pct Recovery = 111%  Analysis Date = 01/18/15 
 Pct Recovery = 111%  Analysis Date = 01/18/15 
 Pct Recovery = 111%  Analysis Date = 01/14/15 
 Pct Recovery = 111%  Analysis Date = 01/14/15 
 Pct Recovery = 111%  Analysis Date = 01/10/15 
 Pct Recovery = 111%  Analysis Date = 01/10/15 
 Pct Recovery = 111%  Analysis Date = 01/06/15 
 Pct Recovery = 111%  Analysis Date = 01/06/15 
 Pct Recovery = 111%  Analysis Date = 01/02/15 
 Pct Recovery = 111%  Analysis Date = 01/02/15 
 Pct Recovery = 111%  Analysis Date = 12/28/14 
 Pct Recovery = 111%  Analysis Date = 12/28/14 
 Pct Recovery = 111%  Analysis Date = 12/24/14 
 Pct Recovery = 111%  Analysis Date = 12/24/14 
 Pct Recovery = 111%  Analysis Date = 12/20/14 
 Pct Recovery = 111%  Analysis Date = 12/20/14 
 Pct Recovery = 111%  Analysis Date = 12/16/14 
 Pct Recovery = 111%  Analysis Date = 12/16/14 
 Pct Recovery = 111%  Analysis Date = 12/12/14 
 Pct Recovery = 111%  Analysis Date = 12/12/14 
 Pct Recovery = 111%  Analysis Date = 12/08/14 
 Pct Recovery = 111%  Analysis Date = 12/08/14 
 Pct Recovery = 111%  Analysis Date = 12/04/14 
 Pct Recovery = 111%  Analysis Date = 12/04/14 
 Pct Recovery = 111%  Analysis Date = 11/29/14 
 Pct Recovery = 111%  Analysis Date = 11/29/14 
 Pct Recovery = 111%  Analysis Date = 11/25/14 
 Pct Recovery = 111%  Analysis Date = 11/25/14 
 Pct Recovery = 111%  Analysis Date = 11/21/14 
 Pct Recovery = 111%  Analysis Date = 11/21/14 
 Pct Recovery = 111%  Analysis Date = 11/17/14 
 Pct Recovery = 111%  Analysis Date = 11/17/14 
 Pct Recovery = 111%  Analysis Date = 11/13/14 
 Pct Recovery = 111%  Analysis Date = 11/13/14 
 Pct Recovery = 111%  Analysis Date = 11/09/14 
 Pct Recovery = 110%  Analysis Date = 11/09/14 
 Pct Recovery = 110%  Analysis Date = 11/05/14 
 Pct Recovery = 110%  Analysis Date = 11/05/14 
 Pct Recovery = 110%  Analysis Date = 11/01/14 
 Pct Recovery = 110%  Analysis Date = 11/01/14 
 Pct Recovery = 110%  Analysis Date = 10/27/14 
 Pct Recovery = 110%  Analysis Date = 10/27/14 
 Pct Recovery = 110%  Analysis Date = 10/23/14 
 Pct Recovery = 110%  Analysis Date = 10/23/14 
 Pct Recovery = 110%  Analysis Date = 10/19/14 
 Pct Recovery = 110%  Analysis Date = 10/19/14 
 Pct Recovery = 110%  Analysis Date = 10/15/14 
 Pct Recovery = 110%  Analysis Date = 10/15/14 
 Pct Recovery = 110%  Analysis Date = 10/11/14 
 Pct Recovery = 110%  Analysis Date = 10/11/14 
 Pct Recovery = 110%  Analysis Date = 10/07/14 
 Pct Recovery = 110%  Analysis Date = 10/07/14 
 Pct Recovery = 110%  Analysis Date = 10/03/14 
 Pct Recovery = 110%  Analysis Date = 10/03/14 
 Pct Recovery = 110%  Analysis Date = 09/28/14 
 Pct Recovery = 110%  Analysis Date = 09/28/14 
 Pct Recovery = 110%  Analysis Date = 09/24/14 
 Pct Recovery = 110%  Analysis Date = 09/24/14 
 Pct Recovery = 110%  Analysis Date = 09/20/14 
 Pct Recovery = 110%  Analysis Date = 09/20/14 
 Pct Recovery = 110%  Analysis Date = 09/16/14 
 Pct Recovery = 110%  Analysis Date = 09/16/14 
 Pct Recovery = 110%  Analysis Date = 09/12/14 
 Pct Recovery = 110%  Analysis Date = 09/12/14 
 Pct Recovery = 110%  Analysis Date = 09/08/14 
 Pct Recovery = 110%  Analysis Date = 09/08/14 
 Pct Recovery = 110%  Analysis Date = 09/04/14 
 Pct Recovery = 110%  Analysis Date = 09/04/14 
 Pct Recovery = 110%  Analysis Date = 08/30/14 
 Pct Recovery = 109%  Analysis Date = 08/30/14 
 Pct Recovery = 109%  Analysis Date = 08/26/14 
 Pct Recovery = 109%  Analysis Date = 08/26/14 
 Pct Recovery = 109%  Analysis Date = 08/22/14 
 Pct Recovery = 109%  Analysis Date = 08/22/14 
 Pct Recovery = 109%  Analysis Date = 08/18/14 
 Pct Recovery = 109%  Analysis Date = 08/18/14 
 Pct Recovery = 109%  Analysis Date = 08/14/14 
 Pct Recovery = 109%  Analysis Date = 08/14/14 
 Pct Recovery = 109%  Analysis Date = 08/10/14 
 Pct Recovery = 109%  Analysis Date = 08/10/14 
 Pct Recovery = 109%  Analysis Date = 08/06/14 
 Pct Recovery = 109%  Analysis Date = 08/06/14 
 Pct Recovery = 109%  Analysis Date = 08/01/14 
 Pct Recovery = 109%  Analysis Date = 08/01/14 
 Pct Recovery = 109%  Analysis Date = 07/28/14 
 Pct Recovery = 109%  Analysis Date = 07/28/14 
 Pct Recovery = 109%  Analysis Date = 07/24/14 
 Pct Recovery = 109%  Analysis Date = 07/24/14 
 Pct Recovery = 109%  Analysis Date = 07/20/14 
 Pct Recovery = 109%  Analysis Date = 07/20/14 
 Pct Recovery = 109%  Analysis Date = 07/16/14 
 Pct Recovery = 109%  Analysis Date = 07/16/14 
 Pct Recovery = 109%  Analysis Date = 07/12/14 
 Pct Recovery = 109%  Analysis Date = 07/12/14 
 Pct Recovery = 109%  Analysis Date = 07/08/14 
 Pct Recovery = 109%  Analysis Date = 07/08/14 
 Pct Recovery = 109%  Analysis Date = 07/03/14 
 Pct Recovery = 109%  Analysis Date = 07/03/14 
 Pct Recovery = 109%  Analysis Date = 06/29/14 
 Pct Recovery = 109%  Analysis Date = 06/29/14 
 Pct Recovery = 109%  Analysis Date = 06/25/14 
 Pct Recovery = 108%  Analysis Date = 06/25/14 
 Pct Recovery = 108%  Analysis Date = 06/21/14 
 Pct Recovery = 108%  Analysis Date = 06/21/14 
 Pct Recovery = 108%  Analysis Date = 06/17/14 
 Pct Recovery = 108%  Analysis Date = 06/17/14 
 Pct Recovery = 108%  Analysis Date = 06/13/14 
 Pct Recovery = 108%  Analysis Date = 06/13/14 
 Pct Recovery = 108%  Analysis Date = 06/09/14 
 Pct Recovery = 108%  Analysis Date = 06/09/14 
 Pct Recovery = 108%  Analysis Date = 06/04/14 
 Pct Recovery = 108%  Analysis Date = 06/04/14 
 Pct Recovery = 108%  Analysis Date = 05/31/14 
 Pct Recovery = 108%  Analysis Date = 05/31/14 
 Pct Recovery = 108%  Analysis Date = 05/27/14 
 Pct Recovery = 108%  Analysis Date = 05/27/14 
 Pct Recovery = 108%  Analysis Date = 05/23/14 
 Pct Recovery = 108%  Analysis Date = 05/23/14 
 Pct Recovery = 108%  Analysis Date = 05/19/14 
 Pct Recovery = 108%  Analysis Date = 05/19/14 
 Pct Recovery = 108%  Analysis Date = 05/15/14 
 Pct Recovery = 108%  Analysis Date = 05/15/14 
 Pct Recovery = 108%  Analysis Date = 05/11/14 
 Pct Recovery = 108%  Analysis Date = 05/11/14 
 Pct Recovery = 108%  Analysis Date = 05/07/14 
 Pct Recovery = 108%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
1,3-DIOXOLANE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 37 106% 18% 101% 16%
Total 37 106% 18% 101% 16%

Sample Statistics
1,3-DIOXOLANE

Characteristic N % % Basis
Plotted 37 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 37 .  
False Negatives 0 0% 0 out of 37
Not Spiked 17 .  
False Positives 0 0% 0 out of 17

BQS OBSP Determination:
1,4-DIOXANE
METHOD: 4437 , TESTIDCODE: 81582GM016
Open Data Set

 Analysis Date = 01/10/15 
 SpikeMix = Abs 032014: 20 µl & ERA 0321-14-05A: 20 µl 
 Pct Recovery = 90%  Analysis Date = 08/13/14 
 SpikeMix = ERA 0321-14-05: 20 µl & Accu 214031128: 20 µl 
 Pct Recovery = 104%  Analysis Date = 08/13/14 
 SpikeMix = ERA 0321-14-05: 20 µl & Accu 214031128: 20 µl 
 Pct Recovery = 104%  Analysis Date = 07/11/14 
 SpikeMix = ChemService 2615700: 20 µl & Accu 214031128: 20 µl 
 Pct Recovery = 94%  Analysis Date = 07/11/14 
 SpikeMix = ChemService 2615700: 20 µl & Accu 214031128: 20 µl 
 Pct Recovery = 94%  Analysis Date = 07/03/14 
 SpikeMix = Abs 032014: 20 µl & ChemService 2615700: 20 µl 
 Pct Recovery = 86%  Analysis Date = 07/03/14 
 SpikeMix = Abs 032014: 20 µl & ChemService 2615700: 20 µl 
 Pct Recovery = 86%  Analysis Date = 06/07/14 
 SpikeMix = ChemService 2615700: 20 µl & Supelco LC06437: 20 µl 
 Pct Recovery = 101%  Analysis Date = 06/07/14 
 SpikeMix = ChemService 2615700: 20 µl & Supelco LC06437: 20 µl 
 Pct Recovery = 101%  Analysis Date = 06/06/14 
 SpikeMix = NSI 031814: 20 µl & ChemService 2615700: 20 µl 
 Pct Recovery = 104%  Analysis Date = 06/06/14 
 SpikeMix = NSI 031814: 20 µl & ChemService 2615700: 20 µl 
 Pct Recovery = 104%  Analysis Date = 10/09/15 
 SpikeMix = Supelco LC13544: 25 µl & NSI 050515HVOC: 25 µl 
 Pct Recovery = 95%  Analysis Date = 10/09/15 
 SpikeMix = ERA 0601-15-05: 25 µl & Accu 215041338: 25 µl 
 Pct Recovery = 88%  Analysis Date = 06/26/15 
 SpikeMix = ChemService 3818700: 25 µl & Accu 215041338: 25 µl 
 Pct Recovery = 85%  Analysis Date = 08/12/16 
 SpikeMix = Accu 216041354: 15 µl & Abs 060916HVOC: 15 µl 
 Pct Recovery = 105%  Analysis Date = 04/28/16 
 SpikeMix = ChemService 3818700: 15 µl & Supelco LC13544: 15 µl 
 Pct Recovery = 95%  Analysis Date = 08/24/15 
 SpikeMix = ERA 0601-15-05: 15 µl & Supelco LC13544: 15 µl 
 Pct Recovery = 95%  Analysis Date = 07/30/15 
 SpikeMix = Supelco LC13544: 15 µl & NSI 050515HVOC: 15 µl 
 Pct Recovery = 102%  Analysis Date = 05/14/15 
 SpikeMix = ChemService 3818700: 15 µl & Supelco LC13544: 15 µl 
 Pct Recovery = 95%  Analysis Date = 11/25/15 
 SpikeMix = Accu 215041338: 15 µl & Abs 040315: 15 µl 
 Pct Recovery = 83%  Analysis Date = 09/05/15 
 SpikeMix = Accu 215041338: 15 µl & NSI 050515HVOC: 15 µl 
 Pct Recovery = 90%  Analysis Date = 04/25/15 
 SpikeMix = Abs 032014: 10 µl & ERA 0321-14-05A: 10 µl 
 Pct Recovery = 108%  Analysis Date = 11/22/14 
 SpikeMix = ChemService 2615700: 10 µl & Supelco LC06437: 10 µl 
 Pct Recovery = 94%  Analysis Date = 10/21/14 
 SpikeMix = ERA 0321-14-05A: 10 µl & Accu 214031128: 10 µl 
 Pct Recovery = 86%  Analysis Date = 09/06/14 
 SpikeMix = ERA 0321-14-05: 10 µl & Supelco LC06437: 10 µl 
 Pct Recovery = 122%  Analysis Date = 09/06/14 
 SpikeMix = ERA 0321-14-05: 10 µl & Supelco LC06437: 10 µl 
 Pct Recovery = 122%  Analysis Date = 07/30/14 
 SpikeMix = NSI 031814: 10 µl & ChemService 2615700: 10 µl 
 Pct Recovery = 94%  Analysis Date = 07/30/14 
 SpikeMix = NSI 031814: 10 µl & ChemService 2615700: 10 µl 
 Pct Recovery = 94%  Analysis Date = 05/20/14 
 SpikeMix = ChemService 2615700: 10 µl & Accu 214031128: 10 µl 
 Pct Recovery = 108%  Analysis Date = 05/20/14 
 SpikeMix = ChemService 2615700: 10 µl & Accu 214031128: 10 µl 
 Pct Recovery = 108%  Analysis Date = 03/22/16 
 SpikeMix = Supelco LC13544: 10 µl & NSI 050515HVOC: 10 µl 
 Pct Recovery = 95%  Analysis Date = 12/10/15 
 SpikeMix = ChemService 3818700: 10 µl & Supelco LC13544: 10 µl 
 Pct Recovery = 95%  Analysis Date = 05/05/15 
 SpikeMix = Supelco LC13544: 10 µl & Abs 040315: 10 µl 
 Pct Recovery = 105%  Analysis Date = 02/12/16 
 SpikeMix = ERA 0601-15-05: 10 µl & Accu 215041338: 10 µl 
 Pct Recovery = 96%  Analysis Date = 01/05/16 
 SpikeMix = Accu 215041338: 10 µl & Abs 040315: 10 µl 
 Pct Recovery = 96%  Analysis Date = 05/20/15 
 SpikeMix = ChemService 3818700: 10 µl & Accu 215041338: 10 µl 
 Pct Recovery = 96%  Analysis Date = 08/12/16 
 Pct Recovery = 98%  Analysis Date = 08/07/16 
 Pct Recovery = 98%  Analysis Date = 08/07/16 
 Pct Recovery = 98%  Analysis Date = 08/03/16 
 Pct Recovery = 98%  Analysis Date = 08/03/16 
 Pct Recovery = 98%  Analysis Date = 07/30/16 
 Pct Recovery = 98%  Analysis Date = 07/30/16 
 Pct Recovery = 98%  Analysis Date = 07/26/16 
 Pct Recovery = 97%  Analysis Date = 07/26/16 
 Pct Recovery = 97%  Analysis Date = 07/22/16 
 Pct Recovery = 97%  Analysis Date = 07/22/16 
 Pct Recovery = 97%  Analysis Date = 07/18/16 
 Pct Recovery = 97%  Analysis Date = 07/18/16 
 Pct Recovery = 97%  Analysis Date = 07/14/16 
 Pct Recovery = 97%  Analysis Date = 07/14/16 
 Pct Recovery = 97%  Analysis Date = 07/10/16 
 Pct Recovery = 97%  Analysis Date = 07/10/16 
 Pct Recovery = 97%  Analysis Date = 07/06/16 
 Pct Recovery = 97%  Analysis Date = 07/06/16 
 Pct Recovery = 97%  Analysis Date = 07/02/16 
 Pct Recovery = 97%  Analysis Date = 07/02/16 
 Pct Recovery = 97%  Analysis Date = 06/28/16 
 Pct Recovery = 97%  Analysis Date = 06/28/16 
 Pct Recovery = 97%  Analysis Date = 06/24/16 
 Pct Recovery = 97%  Analysis Date = 06/24/16 
 Pct Recovery = 97%  Analysis Date = 06/20/16 
 Pct Recovery = 97%  Analysis Date = 06/20/16 
 Pct Recovery = 97%  Analysis Date = 06/15/16 
 Pct Recovery = 97%  Analysis Date = 06/15/16 
 Pct Recovery = 97%  Analysis Date = 06/11/16 
 Pct Recovery = 97%  Analysis Date = 06/11/16 
 Pct Recovery = 97%  Analysis Date = 06/07/16 
 Pct Recovery = 97%  Analysis Date = 06/07/16 
 Pct Recovery = 97%  Analysis Date = 06/03/16 
 Pct Recovery = 97%  Analysis Date = 06/03/16 
 Pct Recovery = 97%  Analysis Date = 05/30/16 
 Pct Recovery = 97%  Analysis Date = 05/30/16 
 Pct Recovery = 97%  Analysis Date = 05/26/16 
 Pct Recovery = 97%  Analysis Date = 05/26/16 
 Pct Recovery = 97%  Analysis Date = 05/22/16 
 Pct Recovery = 97%  Analysis Date = 05/22/16 
 Pct Recovery = 97%  Analysis Date = 05/18/16 
 Pct Recovery = 97%  Analysis Date = 05/18/16 
 Pct Recovery = 97%  Analysis Date = 05/14/16 
 Pct Recovery = 97%  Analysis Date = 05/14/16 
 Pct Recovery = 97%  Analysis Date = 05/10/16 
 Pct Recovery = 97%  Analysis Date = 05/10/16 
 Pct Recovery = 97%  Analysis Date = 05/06/16 
 Pct Recovery = 97%  Analysis Date = 05/06/16 
 Pct Recovery = 97%  Analysis Date = 05/02/16 
 Pct Recovery = 97%  Analysis Date = 05/02/16 
 Pct Recovery = 97%  Analysis Date = 04/28/16 
 Pct Recovery = 96%  Analysis Date = 04/28/16 
 Pct Recovery = 96%  Analysis Date = 04/23/16 
 Pct Recovery = 96%  Analysis Date = 04/23/16 
 Pct Recovery = 96%  Analysis Date = 04/19/16 
 Pct Recovery = 96%  Analysis Date = 04/19/16 
 Pct Recovery = 96%  Analysis Date = 04/15/16 
 Pct Recovery = 96%  Analysis Date = 04/15/16 
 Pct Recovery = 96%  Analysis Date = 04/11/16 
 Pct Recovery = 96%  Analysis Date = 04/11/16 
 Pct Recovery = 96%  Analysis Date = 04/07/16 
 Pct Recovery = 96%  Analysis Date = 04/07/16 
 Pct Recovery = 96%  Analysis Date = 04/03/16 
 Pct Recovery = 96%  Analysis Date = 04/03/16 
 Pct Recovery = 96%  Analysis Date = 03/30/16 
 Pct Recovery = 96%  Analysis Date = 03/30/16 
 Pct Recovery = 96%  Analysis Date = 03/26/16 
 Pct Recovery = 96%  Analysis Date = 03/26/16 
 Pct Recovery = 96%  Analysis Date = 03/22/16 
 Pct Recovery = 96%  Analysis Date = 03/22/16 
 Pct Recovery = 96%  Analysis Date = 03/18/16 
 Pct Recovery = 96%  Analysis Date = 03/18/16 
 Pct Recovery = 96%  Analysis Date = 03/14/16 
 Pct Recovery = 96%  Analysis Date = 03/14/16 
 Pct Recovery = 96%  Analysis Date = 03/10/16 
 Pct Recovery = 96%  Analysis Date = 03/10/16 
 Pct Recovery = 96%  Analysis Date = 03/06/16 
 Pct Recovery = 96%  Analysis Date = 03/06/16 
 Pct Recovery = 96%  Analysis Date = 03/02/16 
 Pct Recovery = 96%  Analysis Date = 03/02/16 
 Pct Recovery = 96%  Analysis Date = 02/26/16 
 Pct Recovery = 96%  Analysis Date = 02/26/16 
 Pct Recovery = 96%  Analysis Date = 02/22/16 
 Pct Recovery = 96%  Analysis Date = 02/22/16 
 Pct Recovery = 96%  Analysis Date = 02/18/16 
 Pct Recovery = 96%  Analysis Date = 02/18/16 
 Pct Recovery = 96%  Analysis Date = 02/14/16 
 Pct Recovery = 96%  Analysis Date = 02/14/16 
 Pct Recovery = 96%  Analysis Date = 02/10/16 
 Pct Recovery = 96%  Analysis Date = 02/10/16 
 Pct Recovery = 96%  Analysis Date = 02/06/16 
 Pct Recovery = 96%  Analysis Date = 02/06/16 
 Pct Recovery = 96%  Analysis Date = 02/02/16 
 Pct Recovery = 95%  Analysis Date = 02/02/16 
 Pct Recovery = 95%  Analysis Date = 01/29/16 
 Pct Recovery = 95%  Analysis Date = 01/29/16 
 Pct Recovery = 95%  Analysis Date = 01/25/16 
 Pct Recovery = 95%  Analysis Date = 01/25/16 
 Pct Recovery = 95%  Analysis Date = 01/21/16 
 Pct Recovery = 95%  Analysis Date = 01/21/16 
 Pct Recovery = 95%  Analysis Date = 01/17/16 
 Pct Recovery = 95%  Analysis Date = 01/17/16 
 Pct Recovery = 95%  Analysis Date = 01/13/16 
 Pct Recovery = 95%  Analysis Date = 01/13/16 
 Pct Recovery = 95%  Analysis Date = 01/09/16 
 Pct Recovery = 95%  Analysis Date = 01/09/16 
 Pct Recovery = 95%  Analysis Date = 01/04/16 
 Pct Recovery = 95%  Analysis Date = 01/04/16 
 Pct Recovery = 95%  Analysis Date = 12/31/15 
 Pct Recovery = 95%  Analysis Date = 12/31/15 
 Pct Recovery = 95%  Analysis Date = 12/27/15 
 Pct Recovery = 95%  Analysis Date = 12/27/15 
 Pct Recovery = 95%  Analysis Date = 12/23/15 
 Pct Recovery = 95%  Analysis Date = 12/23/15 
 Pct Recovery = 95%  Analysis Date = 12/19/15 
 Pct Recovery = 95%  Analysis Date = 12/19/15 
 Pct Recovery = 95%  Analysis Date = 12/15/15 
 Pct Recovery = 95%  Analysis Date = 12/15/15 
 Pct Recovery = 95%  Analysis Date = 12/11/15 
 Pct Recovery = 95%  Analysis Date = 12/11/15 
 Pct Recovery = 95%  Analysis Date = 12/07/15 
 Pct Recovery = 95%  Analysis Date = 12/07/15 
 Pct Recovery = 95%  Analysis Date = 12/03/15 
 Pct Recovery = 95%  Analysis Date = 12/03/15 
 Pct Recovery = 95%  Analysis Date = 11/29/15 
 Pct Recovery = 95%  Analysis Date = 11/29/15 
 Pct Recovery = 95%  Analysis Date = 11/25/15 
 Pct Recovery = 95%  Analysis Date = 11/25/15 
 Pct Recovery = 95%  Analysis Date = 11/21/15 
 Pct Recovery = 95%  Analysis Date = 11/21/15 
 Pct Recovery = 95%  Analysis Date = 11/17/15 
 Pct Recovery = 95%  Analysis Date = 11/17/15 
 Pct Recovery = 95%  Analysis Date = 11/12/15 
 Pct Recovery = 95%  Analysis Date = 11/12/15 
 Pct Recovery = 95%  Analysis Date = 11/08/15 
 Pct Recovery = 95%  Analysis Date = 11/08/15 
 Pct Recovery = 95%  Analysis Date = 11/04/15 
 Pct Recovery = 95%  Analysis Date = 11/04/15 
 Pct Recovery = 95%  Analysis Date = 10/31/15 
 Pct Recovery = 95%  Analysis Date = 10/31/15 
 Pct Recovery = 95%  Analysis Date = 10/27/15 
 Pct Recovery = 95%  Analysis Date = 10/27/15 
 Pct Recovery = 95%  Analysis Date = 10/23/15 
 Pct Recovery = 95%  Analysis Date = 10/23/15 
 Pct Recovery = 95%  Analysis Date = 10/19/15 
 Pct Recovery = 95%  Analysis Date = 10/19/15 
 Pct Recovery = 95%  Analysis Date = 10/15/15 
 Pct Recovery = 95%  Analysis Date = 10/15/15 
 Pct Recovery = 95%  Analysis Date = 10/11/15 
 Pct Recovery = 95%  Analysis Date = 10/11/15 
 Pct Recovery = 95%  Analysis Date = 10/07/15 
 Pct Recovery = 95%  Analysis Date = 10/07/15 
 Pct Recovery = 95%  Analysis Date = 10/03/15 
 Pct Recovery = 95%  Analysis Date = 10/03/15 
 Pct Recovery = 95%  Analysis Date = 09/29/15 
 Pct Recovery = 95%  Analysis Date = 09/29/15 
 Pct Recovery = 95%  Analysis Date = 09/25/15 
 Pct Recovery = 95%  Analysis Date = 09/25/15 
 Pct Recovery = 95%  Analysis Date = 09/21/15 
 Pct Recovery = 95%  Analysis Date = 09/21/15 
 Pct Recovery = 95%  Analysis Date = 09/16/15 
 Pct Recovery = 95%  Analysis Date = 09/16/15 
 Pct Recovery = 95%  Analysis Date = 09/12/15 
 Pct Recovery = 95%  Analysis Date = 09/12/15 
 Pct Recovery = 95%  Analysis Date = 09/08/15 
 Pct Recovery = 95%  Analysis Date = 09/08/15 
 Pct Recovery = 95%  Analysis Date = 09/04/15 
 Pct Recovery = 95%  Analysis Date = 09/04/15 
 Pct Recovery = 95%  Analysis Date = 08/31/15 
 Pct Recovery = 95%  Analysis Date = 08/31/15 
 Pct Recovery = 95%  Analysis Date = 08/27/15 
 Pct Recovery = 95%  Analysis Date = 08/27/15 
 Pct Recovery = 95%  Analysis Date = 08/23/15 
 Pct Recovery = 95%  Analysis Date = 08/23/15 
 Pct Recovery = 95%  Analysis Date = 08/19/15 
 Pct Recovery = 95%  Analysis Date = 08/19/15 
 Pct Recovery = 95%  Analysis Date = 08/15/15 
 Pct Recovery = 95%  Analysis Date = 08/15/15 
 Pct Recovery = 95%  Analysis Date = 08/11/15 
 Pct Recovery = 95%  Analysis Date = 08/11/15 
 Pct Recovery = 95%  Analysis Date = 08/07/15 
 Pct Recovery = 95%  Analysis Date = 08/07/15 
 Pct Recovery = 95%  Analysis Date = 08/03/15 
 Pct Recovery = 95%  Analysis Date = 08/03/15 
 Pct Recovery = 95%  Analysis Date = 07/30/15 
 Pct Recovery = 95%  Analysis Date = 07/30/15 
 Pct Recovery = 95%  Analysis Date = 07/25/15 
 Pct Recovery = 95%  Analysis Date = 07/25/15 
 Pct Recovery = 95%  Analysis Date = 07/21/15 
 Pct Recovery = 95%  Analysis Date = 07/21/15 
 Pct Recovery = 95%  Analysis Date = 07/17/15 
 Pct Recovery = 95%  Analysis Date = 07/17/15 
 Pct Recovery = 95%  Analysis Date = 07/13/15 
 Pct Recovery = 95%  Analysis Date = 07/13/15 
 Pct Recovery = 95%  Analysis Date = 07/09/15 
 Pct Recovery = 95%  Analysis Date = 07/09/15 
 Pct Recovery = 95%  Analysis Date = 07/05/15 
 Pct Recovery = 95%  Analysis Date = 07/05/15 
 Pct Recovery = 95%  Analysis Date = 07/01/15 
 Pct Recovery = 95%  Analysis Date = 07/01/15 
 Pct Recovery = 95%  Analysis Date = 06/27/15 
 Pct Recovery = 95%  Analysis Date = 06/27/15 
 Pct Recovery = 95%  Analysis Date = 06/23/15 
 Pct Recovery = 95%  Analysis Date = 06/23/15 
 Pct Recovery = 95%  Analysis Date = 06/19/15 
 Pct Recovery = 95%  Analysis Date = 06/19/15 
 Pct Recovery = 95%  Analysis Date = 06/15/15 
 Pct Recovery = 95%  Analysis Date = 06/15/15 
 Pct Recovery = 95%  Analysis Date = 06/11/15 
 Pct Recovery = 95%  Analysis Date = 06/11/15 
 Pct Recovery = 95%  Analysis Date = 06/07/15 
 Pct Recovery = 96%  Analysis Date = 06/07/15 
 Pct Recovery = 96%  Analysis Date = 06/02/15 
 Pct Recovery = 96%  Analysis Date = 06/02/15 
 Pct Recovery = 96%  Analysis Date = 05/29/15 
 Pct Recovery = 96%  Analysis Date = 05/29/15 
 Pct Recovery = 96%  Analysis Date = 05/25/15 
 Pct Recovery = 96%  Analysis Date = 05/25/15 
 Pct Recovery = 96%  Analysis Date = 05/21/15 
 Pct Recovery = 96%  Analysis Date = 05/21/15 
 Pct Recovery = 96%  Analysis Date = 05/17/15 
 Pct Recovery = 96%  Analysis Date = 05/17/15 
 Pct Recovery = 96%  Analysis Date = 05/13/15 
 Pct Recovery = 96%  Analysis Date = 05/13/15 
 Pct Recovery = 96%  Analysis Date = 05/09/15 
 Pct Recovery = 96%  Analysis Date = 05/09/15 
 Pct Recovery = 96%  Analysis Date = 05/05/15 
 Pct Recovery = 96%  Analysis Date = 05/05/15 
 Pct Recovery = 96%  Analysis Date = 05/01/15 
 Pct Recovery = 96%  Analysis Date = 05/01/15 
 Pct Recovery = 96%  Analysis Date = 04/27/15 
 Pct Recovery = 96%  Analysis Date = 04/27/15 
 Pct Recovery = 96%  Analysis Date = 04/23/15 
 Pct Recovery = 96%  Analysis Date = 04/23/15 
 Pct Recovery = 96%  Analysis Date = 04/19/15 
 Pct Recovery = 96%  Analysis Date = 04/19/15 
 Pct Recovery = 96%  Analysis Date = 04/15/15 
 Pct Recovery = 96%  Analysis Date = 04/15/15 
 Pct Recovery = 96%  Analysis Date = 04/11/15 
 Pct Recovery = 96%  Analysis Date = 04/11/15 
 Pct Recovery = 96%  Analysis Date = 04/06/15 
 Pct Recovery = 96%  Analysis Date = 04/06/15 
 Pct Recovery = 96%  Analysis Date = 04/02/15 
 Pct Recovery = 96%  Analysis Date = 04/02/15 
 Pct Recovery = 96%  Analysis Date = 03/29/15 
 Pct Recovery = 96%  Analysis Date = 03/29/15 
 Pct Recovery = 96%  Analysis Date = 03/25/15 
 Pct Recovery = 96%  Analysis Date = 03/25/15 
 Pct Recovery = 96%  Analysis Date = 03/21/15 
 Pct Recovery = 96%  Analysis Date = 03/21/15 
 Pct Recovery = 96%  Analysis Date = 03/17/15 
 Pct Recovery = 96%  Analysis Date = 03/17/15 
 Pct Recovery = 96%  Analysis Date = 03/13/15 
 Pct Recovery = 96%  Analysis Date = 03/13/15 
 Pct Recovery = 96%  Analysis Date = 03/09/15 
 Pct Recovery = 96%  Analysis Date = 03/09/15 
 Pct Recovery = 96%  Analysis Date = 03/05/15 
 Pct Recovery = 96%  Analysis Date = 03/05/15 
 Pct Recovery = 96%  Analysis Date = 03/01/15 
 Pct Recovery = 96%  Analysis Date = 03/01/15 
 Pct Recovery = 96%  Analysis Date = 02/25/15 
 Pct Recovery = 96%  Analysis Date = 02/25/15 
 Pct Recovery = 96%  Analysis Date = 02/21/15 
 Pct Recovery = 96%  Analysis Date = 02/21/15 
 Pct Recovery = 96%  Analysis Date = 02/17/15 
 Pct Recovery = 96%  Analysis Date = 02/17/15 
 Pct Recovery = 96%  Analysis Date = 02/12/15 
 Pct Recovery = 96%  Analysis Date = 02/12/15 
 Pct Recovery = 96%  Analysis Date = 02/08/15 
 Pct Recovery = 96%  Analysis Date = 02/08/15 
 Pct Recovery = 96%  Analysis Date = 02/04/15 
 Pct Recovery = 96%  Analysis Date = 02/04/15 
 Pct Recovery = 96%  Analysis Date = 01/31/15 
 Pct Recovery = 96%  Analysis Date = 01/31/15 
 Pct Recovery = 96%  Analysis Date = 01/27/15 
 Pct Recovery = 96%  Analysis Date = 01/27/15 
 Pct Recovery = 96%  Analysis Date = 01/23/15 
 Pct Recovery = 96%  Analysis Date = 01/23/15 
 Pct Recovery = 96%  Analysis Date = 01/19/15 
 Pct Recovery = 96%  Analysis Date = 01/19/15 
 Pct Recovery = 96%  Analysis Date = 01/15/15 
 Pct Recovery = 96%  Analysis Date = 01/15/15 
 Pct Recovery = 96%  Analysis Date = 01/11/15 
 Pct Recovery = 96%  Analysis Date = 01/11/15 
 Pct Recovery = 96%  Analysis Date = 01/07/15 
 Pct Recovery = 96%  Analysis Date = 01/07/15 
 Pct Recovery = 96%  Analysis Date = 01/03/15 
 Pct Recovery = 96%  Analysis Date = 01/03/15 
 Pct Recovery = 96%  Analysis Date = 12/30/14 
 Pct Recovery = 96%  Analysis Date = 12/30/14 
 Pct Recovery = 96%  Analysis Date = 12/26/14 
 Pct Recovery = 96%  Analysis Date = 12/26/14 
 Pct Recovery = 96%  Analysis Date = 12/21/14 
 Pct Recovery = 96%  Analysis Date = 12/21/14 
 Pct Recovery = 96%  Analysis Date = 12/17/14 
 Pct Recovery = 96%  Analysis Date = 12/17/14 
 Pct Recovery = 96%  Analysis Date = 12/13/14 
 Pct Recovery = 96%  Analysis Date = 12/13/14 
 Pct Recovery = 96%  Analysis Date = 12/09/14 
 Pct Recovery = 96%  Analysis Date = 12/09/14 
 Pct Recovery = 96%  Analysis Date = 12/05/14 
 Pct Recovery = 96%  Analysis Date = 12/05/14 
 Pct Recovery = 96%  Analysis Date = 12/01/14 
 Pct Recovery = 96%  Analysis Date = 12/01/14 
 Pct Recovery = 96%  Analysis Date = 11/27/14 
 Pct Recovery = 96%  Analysis Date = 11/27/14 
 Pct Recovery = 96%  Analysis Date = 11/23/14 
 Pct Recovery = 96%  Analysis Date = 11/23/14 
 Pct Recovery = 96%  Analysis Date = 11/19/14 
 Pct Recovery = 96%  Analysis Date = 11/19/14 
 Pct Recovery = 96%  Analysis Date = 11/15/14 
 Pct Recovery = 97%  Analysis Date = 11/15/14 
 Pct Recovery = 97%  Analysis Date = 11/11/14 
 Pct Recovery = 97%  Analysis Date = 11/11/14 
 Pct Recovery = 97%  Analysis Date = 11/07/14 
 Pct Recovery = 97%  Analysis Date = 11/07/14 
 Pct Recovery = 97%  Analysis Date = 11/03/14 
 Pct Recovery = 97%  Analysis Date = 11/03/14 
 Pct Recovery = 97%  Analysis Date = 10/30/14 
 Pct Recovery = 97%  Analysis Date = 10/30/14 
 Pct Recovery = 97%  Analysis Date = 10/25/14 
 Pct Recovery = 97%  Analysis Date = 10/25/14 
 Pct Recovery = 97%  Analysis Date = 10/21/14 
 Pct Recovery = 97%  Analysis Date = 10/21/14 
 Pct Recovery = 97%  Analysis Date = 10/17/14 
 Pct Recovery = 98%  Analysis Date = 10/17/14 
 Pct Recovery = 98%  Analysis Date = 10/13/14 
 Pct Recovery = 98%  Analysis Date = 10/13/14 
 Pct Recovery = 98%  Analysis Date = 10/09/14 
 Pct Recovery = 98%  Analysis Date = 10/09/14 
 Pct Recovery = 98%  Analysis Date = 10/05/14 
 Pct Recovery = 98%  Analysis Date = 10/05/14 
 Pct Recovery = 98%  Analysis Date = 10/01/14 
 Pct Recovery = 98%  Analysis Date = 10/01/14 
 Pct Recovery = 98%  Analysis Date = 09/27/14 
 Pct Recovery = 98%  Analysis Date = 09/27/14 
 Pct Recovery = 98%  Analysis Date = 09/23/14 
 Pct Recovery = 98%  Analysis Date = 09/23/14 
 Pct Recovery = 98%  Analysis Date = 09/19/14 
 Pct Recovery = 98%  Analysis Date = 09/19/14 
 Pct Recovery = 98%  Analysis Date = 09/15/14 
 Pct Recovery = 99%  Analysis Date = 09/15/14 
 Pct Recovery = 99%  Analysis Date = 09/11/14 
 Pct Recovery = 99%  Analysis Date = 09/11/14 
 Pct Recovery = 99%  Analysis Date = 09/07/14 
 Pct Recovery = 99%  Analysis Date = 09/07/14 
 Pct Recovery = 99%  Analysis Date = 09/02/14 
 Pct Recovery = 99%  Analysis Date = 09/02/14 
 Pct Recovery = 99%  Analysis Date = 08/29/14 
 Pct Recovery = 99%  Analysis Date = 08/29/14 
 Pct Recovery = 99%  Analysis Date = 08/25/14 
 Pct Recovery = 99%  Analysis Date = 08/25/14 
 Pct Recovery = 99%  Analysis Date = 08/21/14 
 Pct Recovery = 99%  Analysis Date = 08/21/14 
 Pct Recovery = 99%  Analysis Date = 08/17/14 
 Pct Recovery = 99%  Analysis Date = 08/17/14 
 Pct Recovery = 99%  Analysis Date = 08/13/14 
 Pct Recovery = 100%  Analysis Date = 08/13/14 
 Pct Recovery = 100%  Analysis Date = 08/09/14 
 Pct Recovery = 100%  Analysis Date = 08/09/14 
 Pct Recovery = 100%  Analysis Date = 08/05/14 
 Pct Recovery = 100%  Analysis Date = 08/05/14 
 Pct Recovery = 100%  Analysis Date = 08/01/14 
 Pct Recovery = 100%  Analysis Date = 08/01/14 
 Pct Recovery = 100%  Analysis Date = 07/28/14 
 Pct Recovery = 100%  Analysis Date = 07/28/14 
 Pct Recovery = 100%  Analysis Date = 07/24/14 
 Pct Recovery = 100%  Analysis Date = 07/24/14 
 Pct Recovery = 100%  Analysis Date = 07/20/14 
 Pct Recovery = 100%  Analysis Date = 07/20/14 
 Pct Recovery = 100%  Analysis Date = 07/16/14 
 Pct Recovery = 100%  Analysis Date = 07/16/14 
 Pct Recovery = 100%  Analysis Date = 07/11/14 
 Pct Recovery = 100%  Analysis Date = 07/11/14 
 Pct Recovery = 100%  Analysis Date = 07/07/14 
 Pct Recovery = 101%  Analysis Date = 07/07/14 
 Pct Recovery = 101%  Analysis Date = 07/03/14 
 Pct Recovery = 101%  Analysis Date = 07/03/14 
 Pct Recovery = 101%  Analysis Date = 06/29/14 
 Pct Recovery = 101%  Analysis Date = 06/29/14 
 Pct Recovery = 101%  Analysis Date = 06/25/14 
 Pct Recovery = 101%  Analysis Date = 06/25/14 
 Pct Recovery = 101%  Analysis Date = 06/21/14 
 Pct Recovery = 101%  Analysis Date = 06/21/14 
 Pct Recovery = 101%  Analysis Date = 06/17/14 
 Pct Recovery = 101%  Analysis Date = 06/17/14 
 Pct Recovery = 101%  Analysis Date = 06/13/14 
 Pct Recovery = 101%  Analysis Date = 06/13/14 
 Pct Recovery = 101%  Analysis Date = 06/09/14 
 Pct Recovery = 101%  Analysis Date = 06/09/14 
 Pct Recovery = 101%  Analysis Date = 06/05/14 
 Pct Recovery = 101%  Analysis Date = 06/05/14 
 Pct Recovery = 101%  Analysis Date = 06/01/14 
 Pct Recovery = 101%  Analysis Date = 06/01/14 
 Pct Recovery = 101%  Analysis Date = 05/28/14 
 Pct Recovery = 101%  Analysis Date = 05/28/14 
 Pct Recovery = 101%  Analysis Date = 05/24/14 
 Pct Recovery = 101%  Analysis Date = 05/24/14 
 Pct Recovery = 101%  Analysis Date = 05/20/14 
 Pct Recovery = 101%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
1,4-DIOXANE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 36 98% 9% 95% 8%
Total 36 98% 9% 95% 8%

Sample Statistics
1,4-DIOXANE

Characteristic N % % Basis
Plotted 36 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 36 .  
False Negatives 0 0% 0 out of 36
Not Spiked 25 .  
False Positives 0 0% 0 out of 25

BQS OBSP Determination:
1-OCTANOL
METHOD: 4437 , TESTIDCODE: 77310GM016
Open Data Set

 Analysis Date = 07/29/16 
 SpikeMix = Supelco LC20145V: 40 µl & NSI 041516: 40 µl & NSI 041416HVOC: 40 µl 
 Pct Recovery = 85%  Analysis Date = 07/06/16 
 SpikeMix = Accu 216041354: 40 µl & NSI 041516: 40 µl & NSI 041416HVOC: 40 µl 
 Pct Recovery = 76%  Analysis Date = 06/29/16 
 SpikeMix = NSI 041516: 40 µl & ChemService 5082800: 40 µl 
 Pct Recovery = 81%  Analysis Date = 07/14/16 
 SpikeMix = NSI 041516: 25 µl & ChemService 5082800: 25 µl & NSI 041416HVOC: 25 µl 
 Pct Recovery = 67%  Analysis Date = 05/21/16 
 SpikeMix = Supelco LC20145V: 25 µl & NSI 041516: 25 µl & NSI 041416HVOC: 25 µl 
 Pct Recovery = 80%  Analysis Date = 08/13/14 
 SpikeMix = ERA 0321-14-05: 20 µl & Accu 214031128: 20 µl 
 Pct Recovery = 83%  Analysis Date = 07/23/14 
 SpikeMix = Accu 214031128: 20 µl & Abs 032014: 20 µl 
 Pct Recovery = 83%  Analysis Date = 07/11/14 
 SpikeMix = ChemService 2615700: 20 µl & Accu 214031128: 20 µl 
 Pct Recovery = 90%  Analysis Date = 05/07/14 
 SpikeMix = NSI 031814: 20 µl & Accu 214031128: 20 µl 
 Pct Recovery = 88%  Analysis Date = 03/19/15 
 SpikeMix = Supelco LC06437: 20 µl & NSI 031814: 20 µl 
 Pct Recovery = 97%  Analysis Date = 08/20/14 
 SpikeMix = Supelco LC06437: 20 µl & Abs 032014: 20 µl 
 Pct Recovery = 102%  Analysis Date = 06/07/14 
 SpikeMix = ChemService 2615700: 20 µl & Supelco LC06437: 20 µl 
 Pct Recovery = 82%  Analysis Date = 06/26/15 
 SpikeMix = ChemService 3818700: 25 µl & Accu 215041338: 25 µl 
 Pct Recovery = 87%  Analysis Date = 06/25/15 
 SpikeMix = ChemService 3818700: 25 µl & NSI 050515HVOC: 25 µl 
 Pct Recovery = 77%  Analysis Date = 01/22/16 
 SpikeMix = NSI 050515HVOC: 25 µl & ERA 0601-15-05: 25 µl 
 Pct Recovery = 73%  Analysis Date = 10/09/15 
 SpikeMix = ERA 0601-15-05: 25 µl & Accu 215041338: 25 µl 
 Pct Recovery = 83%  Analysis Date = 08/12/16 
 SpikeMix = Accu 216041354: 15 µl & Abs 060916HVOC: 15 µl 
 Pct Recovery = 87%  Analysis Date = 06/03/16 
 SpikeMix = NSI 041516: 15 µl & Phenova B20160303: 15 µl & NSI 041416HVOC: 15 µl 
 Pct Recovery = 83%  Analysis Date = 05/20/16 
 SpikeMix = Accu 216041354: 15 µl & NSI 041516: 15 µl & Accu 216041225: 15 µl 
 Pct Recovery = 79%  Analysis Date = 04/28/16 
 SpikeMix = ChemService 3818700: 15 µl & Supelco LC13544: 15 µl 
 Pct Recovery = 90%  Analysis Date = 06/16/15 
 SpikeMix = ChemService 3818700: 15 µl & NSI 050515HVOC: 15 µl 
 Pct Recovery = 81%  Analysis Date = 05/14/15 
 SpikeMix = ChemService 3818700: 15 µl & Supelco LC13544: 15 µl 
 Pct Recovery = 96%  Analysis Date = 09/24/15 
 SpikeMix = Abs 040315: 15 µl & ERA 0601-15-05: 15 µl 
 Pct Recovery = 74%  Analysis Date = 08/24/15 
 SpikeMix = ERA 0601-15-05: 15 µl & Supelco LC13544: 15 µl 
 Pct Recovery = 89%  Analysis Date = 12/13/14 
 SpikeMix = Accu 214031128: 10 µl & NSI 031814: 10 µl 
 Pct Recovery = 95%  Analysis Date = 10/21/14 
 SpikeMix = ERA 0321-14-05A: 10 µl & Accu 214031128: 10 µl 
 Pct Recovery = 92%  Analysis Date = 09/11/14 
 SpikeMix = Accu 214031128: 10 µl & Abs 032014: 10 µl 
 Pct Recovery = 74%  Analysis Date = 05/20/14 
 SpikeMix = ChemService 2615700: 10 µl & Accu 214031128: 10 µl 
 Pct Recovery = 104%  Analysis Date = 11/22/14 
 SpikeMix = ChemService 2615700: 10 µl & Supelco LC06437: 10 µl 
 Pct Recovery = 88%  Analysis Date = 09/06/14 
 SpikeMix = ERA 0321-14-05: 10 µl & Supelco LC06437: 10 µl 
 Pct Recovery = 94%  Analysis Date = 06/17/14 
 SpikeMix = Supelco LC06437: 10 µl & Abs 032014: 10 µl 
 Pct Recovery = 98%  Analysis Date = 04/09/16 
 SpikeMix = Abs 040315: 10 µl & ChemService 3818700: 10 µl 
 Pct Recovery = 79%  Analysis Date = 12/10/15 
 SpikeMix = ChemService 3818700: 10 µl & Supelco LC13544: 10 µl 
 Pct Recovery = 95%  Analysis Date = 10/23/15 
 SpikeMix = Abs 040315: 10 µl & ChemService 3818700: 10 µl 
 Pct Recovery = 88%  Analysis Date = 05/20/15 
 SpikeMix = ChemService 3818700: 10 µl & Accu 215041338: 10 µl 
 Pct Recovery = 96%  Analysis Date = 02/12/16 
 SpikeMix = ERA 0601-15-05: 10 µl & Accu 215041338: 10 µl 
 Pct Recovery = 84%  Analysis Date = 12/05/15 
 SpikeMix = NSI 050515HVOC: 10 µl & ERA 0601-15-05: 10 µl 
 Pct Recovery = 85%  Analysis Date = 11/14/15 
 SpikeMix = ERA 0601-15-05: 10 µl 
 Pct Recovery = 86%  Analysis Date = 08/14/15 
 SpikeMix = Abs 040315: 10 µl & ERA 0601-15-05: 10 µl 
 Pct Recovery = 72%  Analysis Date = 08/11/16 
 Pct Recovery = 80%  Analysis Date = 08/07/16 
 Pct Recovery = 80%  Analysis Date = 08/07/16 
 Pct Recovery = 80%  Analysis Date = 08/03/16 
 Pct Recovery = 80%  Analysis Date = 08/03/16 
 Pct Recovery = 80%  Analysis Date = 07/30/16 
 Pct Recovery = 80%  Analysis Date = 07/30/16 
 Pct Recovery = 80%  Analysis Date = 07/26/16 
 Pct Recovery = 80%  Analysis Date = 07/26/16 
 Pct Recovery = 80%  Analysis Date = 07/22/16 
 Pct Recovery = 80%  Analysis Date = 07/22/16 
 Pct Recovery = 80%  Analysis Date = 07/18/16 
 Pct Recovery = 80%  Analysis Date = 07/18/16 
 Pct Recovery = 80%  Analysis Date = 07/14/16 
 Pct Recovery = 80%  Analysis Date = 07/14/16 
 Pct Recovery = 80%  Analysis Date = 07/09/16 
 Pct Recovery = 80%  Analysis Date = 07/09/16 
 Pct Recovery = 80%  Analysis Date = 07/05/16 
 Pct Recovery = 80%  Analysis Date = 07/05/16 
 Pct Recovery = 80%  Analysis Date = 07/01/16 
 Pct Recovery = 80%  Analysis Date = 07/01/16 
 Pct Recovery = 80%  Analysis Date = 06/27/16 
 Pct Recovery = 80%  Analysis Date = 06/27/16 
 Pct Recovery = 80%  Analysis Date = 06/23/16 
 Pct Recovery = 81%  Analysis Date = 06/23/16 
 Pct Recovery = 81%  Analysis Date = 06/19/16 
 Pct Recovery = 81%  Analysis Date = 06/19/16 
 Pct Recovery = 81%  Analysis Date = 06/15/16 
 Pct Recovery = 81%  Analysis Date = 06/15/16 
 Pct Recovery = 81%  Analysis Date = 06/10/16 
 Pct Recovery = 81%  Analysis Date = 06/10/16 
 Pct Recovery = 81%  Analysis Date = 06/06/16 
 Pct Recovery = 81%  Analysis Date = 06/06/16 
 Pct Recovery = 81%  Analysis Date = 06/02/16 
 Pct Recovery = 81%  Analysis Date = 06/02/16 
 Pct Recovery = 81%  Analysis Date = 05/29/16 
 Pct Recovery = 81%  Analysis Date = 05/29/16 
 Pct Recovery = 81%  Analysis Date = 05/25/16 
 Pct Recovery = 81%  Analysis Date = 05/25/16 
 Pct Recovery = 81%  Analysis Date = 05/21/16 
 Pct Recovery = 81%  Analysis Date = 05/21/16 
 Pct Recovery = 81%  Analysis Date = 05/17/16 
 Pct Recovery = 81%  Analysis Date = 05/17/16 
 Pct Recovery = 81%  Analysis Date = 05/12/16 
 Pct Recovery = 81%  Analysis Date = 05/12/16 
 Pct Recovery = 81%  Analysis Date = 05/08/16 
 Pct Recovery = 81%  Analysis Date = 05/08/16 
 Pct Recovery = 81%  Analysis Date = 05/04/16 
 Pct Recovery = 81%  Analysis Date = 05/04/16 
 Pct Recovery = 81%  Analysis Date = 04/30/16 
 Pct Recovery = 81%  Analysis Date = 04/30/16 
 Pct Recovery = 81%  Analysis Date = 04/26/16 
 Pct Recovery = 81%  Analysis Date = 04/26/16 
 Pct Recovery = 81%  Analysis Date = 04/22/16 
 Pct Recovery = 81%  Analysis Date = 04/22/16 
 Pct Recovery = 81%  Analysis Date = 04/18/16 
 Pct Recovery = 82%  Analysis Date = 04/18/16 
 Pct Recovery = 82%  Analysis Date = 04/13/16 
 Pct Recovery = 82%  Analysis Date = 04/13/16 
 Pct Recovery = 82%  Analysis Date = 04/09/16 
 Pct Recovery = 82%  Analysis Date = 04/09/16 
 Pct Recovery = 82%  Analysis Date = 04/05/16 
 Pct Recovery = 82%  Analysis Date = 04/05/16 
 Pct Recovery = 82%  Analysis Date = 04/01/16 
 Pct Recovery = 82%  Analysis Date = 04/01/16 
 Pct Recovery = 82%  Analysis Date = 03/28/16 
 Pct Recovery = 82%  Analysis Date = 03/28/16 
 Pct Recovery = 82%  Analysis Date = 03/24/16 
 Pct Recovery = 82%  Analysis Date = 03/24/16 
 Pct Recovery = 82%  Analysis Date = 03/20/16 
 Pct Recovery = 82%  Analysis Date = 03/20/16 
 Pct Recovery = 82%  Analysis Date = 03/15/16 
 Pct Recovery = 82%  Analysis Date = 03/15/16 
 Pct Recovery = 82%  Analysis Date = 03/11/16 
 Pct Recovery = 82%  Analysis Date = 03/11/16 
 Pct Recovery = 82%  Analysis Date = 03/07/16 
 Pct Recovery = 82%  Analysis Date = 03/07/16 
 Pct Recovery = 82%  Analysis Date = 03/03/16 
 Pct Recovery = 82%  Analysis Date = 03/03/16 
 Pct Recovery = 82%  Analysis Date = 02/28/16 
 Pct Recovery = 82%  Analysis Date = 02/28/16 
 Pct Recovery = 82%  Analysis Date = 02/24/16 
 Pct Recovery = 82%  Analysis Date = 02/24/16 
 Pct Recovery = 82%  Analysis Date = 02/20/16 
 Pct Recovery = 83%  Analysis Date = 02/20/16 
 Pct Recovery = 83%  Analysis Date = 02/15/16 
 Pct Recovery = 83%  Analysis Date = 02/15/16 
 Pct Recovery = 83%  Analysis Date = 02/11/16 
 Pct Recovery = 83%  Analysis Date = 02/11/16 
 Pct Recovery = 83%  Analysis Date = 02/07/16 
 Pct Recovery = 83%  Analysis Date = 02/07/16 
 Pct Recovery = 83%  Analysis Date = 02/03/16 
 Pct Recovery = 83%  Analysis Date = 02/03/16 
 Pct Recovery = 83%  Analysis Date = 01/30/16 
 Pct Recovery = 83%  Analysis Date = 01/30/16 
 Pct Recovery = 83%  Analysis Date = 01/26/16 
 Pct Recovery = 83%  Analysis Date = 01/26/16 
 Pct Recovery = 83%  Analysis Date = 01/22/16 
 Pct Recovery = 83%  Analysis Date = 01/22/16 
 Pct Recovery = 83%  Analysis Date = 01/17/16 
 Pct Recovery = 83%  Analysis Date = 01/17/16 
 Pct Recovery = 83%  Analysis Date = 01/13/16 
 Pct Recovery = 83%  Analysis Date = 01/13/16 
 Pct Recovery = 83%  Analysis Date = 01/09/16 
 Pct Recovery = 83%  Analysis Date = 01/09/16 
 Pct Recovery = 83%  Analysis Date = 01/05/16 
 Pct Recovery = 83%  Analysis Date = 01/05/16 
 Pct Recovery = 83%  Analysis Date = 01/01/16 
 Pct Recovery = 83%  Analysis Date = 01/01/16 
 Pct Recovery = 83%  Analysis Date = 12/28/15 
 Pct Recovery = 83%  Analysis Date = 12/28/15 
 Pct Recovery = 83%  Analysis Date = 12/24/15 
 Pct Recovery = 83%  Analysis Date = 12/24/15 
 Pct Recovery = 83%  Analysis Date = 12/20/15 
 Pct Recovery = 83%  Analysis Date = 12/20/15 
 Pct Recovery = 83%  Analysis Date = 12/15/15 
 Pct Recovery = 83%  Analysis Date = 12/15/15 
 Pct Recovery = 83%  Analysis Date = 12/11/15 
 Pct Recovery = 83%  Analysis Date = 12/11/15 
 Pct Recovery = 83%  Analysis Date = 12/07/15 
 Pct Recovery = 83%  Analysis Date = 12/07/15 
 Pct Recovery = 83%  Analysis Date = 12/03/15 
 Pct Recovery = 83%  Analysis Date = 12/03/15 
 Pct Recovery = 83%  Analysis Date = 11/29/15 
 Pct Recovery = 83%  Analysis Date = 11/29/15 
 Pct Recovery = 83%  Analysis Date = 11/25/15 
 Pct Recovery = 83%  Analysis Date = 11/25/15 
 Pct Recovery = 83%  Analysis Date = 11/21/15 
 Pct Recovery = 83%  Analysis Date = 11/21/15 
 Pct Recovery = 83%  Analysis Date = 11/16/15 
 Pct Recovery = 83%  Analysis Date = 11/16/15 
 Pct Recovery = 83%  Analysis Date = 11/12/15 
 Pct Recovery = 83%  Analysis Date = 11/12/15 
 Pct Recovery = 83%  Analysis Date = 11/08/15 
 Pct Recovery = 83%  Analysis Date = 11/08/15 
 Pct Recovery = 83%  Analysis Date = 11/04/15 
 Pct Recovery = 83%  Analysis Date = 11/04/15 
 Pct Recovery = 83%  Analysis Date = 10/31/15 
 Pct Recovery = 83%  Analysis Date = 10/31/15 
 Pct Recovery = 83%  Analysis Date = 10/27/15 
 Pct Recovery = 84%  Analysis Date = 10/27/15 
 Pct Recovery = 84%  Analysis Date = 10/23/15 
 Pct Recovery = 84%  Analysis Date = 10/23/15 
 Pct Recovery = 84%  Analysis Date = 10/18/15 
 Pct Recovery = 84%  Analysis Date = 10/18/15 
 Pct Recovery = 84%  Analysis Date = 10/14/15 
 Pct Recovery = 84%  Analysis Date = 10/14/15 
 Pct Recovery = 84%  Analysis Date = 10/10/15 
 Pct Recovery = 84%  Analysis Date = 10/10/15 
 Pct Recovery = 84%  Analysis Date = 10/06/15 
 Pct Recovery = 84%  Analysis Date = 10/06/15 
 Pct Recovery = 84%  Analysis Date = 10/02/15 
 Pct Recovery = 84%  Analysis Date = 10/02/15 
 Pct Recovery = 84%  Analysis Date = 09/28/15 
 Pct Recovery = 84%  Analysis Date = 09/28/15 
 Pct Recovery = 84%  Analysis Date = 09/24/15 
 Pct Recovery = 84%  Analysis Date = 09/24/15 
 Pct Recovery = 84%  Analysis Date = 09/19/15 
 Pct Recovery = 84%  Analysis Date = 09/19/15 
 Pct Recovery = 84%  Analysis Date = 09/15/15 
 Pct Recovery = 85%  Analysis Date = 09/15/15 
 Pct Recovery = 85%  Analysis Date = 09/11/15 
 Pct Recovery = 85%  Analysis Date = 09/11/15 
 Pct Recovery = 85%  Analysis Date = 09/07/15 
 Pct Recovery = 85%  Analysis Date = 09/07/15 
 Pct Recovery = 85%  Analysis Date = 09/03/15 
 Pct Recovery = 85%  Analysis Date = 09/03/15 
 Pct Recovery = 85%  Analysis Date = 08/30/15 
 Pct Recovery = 85%  Analysis Date = 08/30/15 
 Pct Recovery = 85%  Analysis Date = 08/26/15 
 Pct Recovery = 85%  Analysis Date = 08/26/15 
 Pct Recovery = 85%  Analysis Date = 08/21/15 
 Pct Recovery = 85%  Analysis Date = 08/21/15 
 Pct Recovery = 85%  Analysis Date = 08/17/15 
 Pct Recovery = 85%  Analysis Date = 08/17/15 
 Pct Recovery = 85%  Analysis Date = 08/13/15 
 Pct Recovery = 85%  Analysis Date = 08/13/15 
 Pct Recovery = 85%  Analysis Date = 08/09/15 
 Pct Recovery = 86%  Analysis Date = 08/09/15 
 Pct Recovery = 86%  Analysis Date = 08/05/15 
 Pct Recovery = 86%  Analysis Date = 08/05/15 
 Pct Recovery = 86%  Analysis Date = 08/01/15 
 Pct Recovery = 86%  Analysis Date = 08/01/15 
 Pct Recovery = 86%  Analysis Date = 07/28/15 
 Pct Recovery = 86%  Analysis Date = 07/28/15 
 Pct Recovery = 86%  Analysis Date = 07/23/15 
 Pct Recovery = 86%  Analysis Date = 07/23/15 
 Pct Recovery = 86%  Analysis Date = 07/19/15 
 Pct Recovery = 86%  Analysis Date = 07/19/15 
 Pct Recovery = 86%  Analysis Date = 07/15/15 
 Pct Recovery = 86%  Analysis Date = 07/15/15 
 Pct Recovery = 86%  Analysis Date = 07/11/15 
 Pct Recovery = 86%  Analysis Date = 07/11/15 
 Pct Recovery = 86%  Analysis Date = 07/07/15 
 Pct Recovery = 86%  Analysis Date = 07/07/15 
 Pct Recovery = 86%  Analysis Date = 07/03/15 
 Pct Recovery = 87%  Analysis Date = 07/03/15 
 Pct Recovery = 87%  Analysis Date = 06/29/15 
 Pct Recovery = 87%  Analysis Date = 06/29/15 
 Pct Recovery = 87%  Analysis Date = 06/24/15 
 Pct Recovery = 87%  Analysis Date = 06/24/15 
 Pct Recovery = 87%  Analysis Date = 06/20/15 
 Pct Recovery = 87%  Analysis Date = 06/20/15 
 Pct Recovery = 87%  Analysis Date = 06/16/15 
 Pct Recovery = 87%  Analysis Date = 06/16/15 
 Pct Recovery = 87%  Analysis Date = 06/12/15 
 Pct Recovery = 87%  Analysis Date = 06/12/15 
 Pct Recovery = 87%  Analysis Date = 06/08/15 
 Pct Recovery = 87%  Analysis Date = 06/08/15 
 Pct Recovery = 87%  Analysis Date = 06/04/15 
 Pct Recovery = 87%  Analysis Date = 06/04/15 
 Pct Recovery = 87%  Analysis Date = 05/31/15 
 Pct Recovery = 87%  Analysis Date = 05/31/15 
 Pct Recovery = 87%  Analysis Date = 05/27/15 
 Pct Recovery = 88%  Analysis Date = 05/27/15 
 Pct Recovery = 88%  Analysis Date = 05/22/15 
 Pct Recovery = 88%  Analysis Date = 05/22/15 
 Pct Recovery = 88%  Analysis Date = 05/18/15 
 Pct Recovery = 88%  Analysis Date = 05/18/15 
 Pct Recovery = 88%  Analysis Date = 05/14/15 
 Pct Recovery = 88%  Analysis Date = 05/14/15 
 Pct Recovery = 88%  Analysis Date = 05/10/15 
 Pct Recovery = 88%  Analysis Date = 05/10/15 
 Pct Recovery = 88%  Analysis Date = 05/06/15 
 Pct Recovery = 88%  Analysis Date = 05/06/15 
 Pct Recovery = 88%  Analysis Date = 05/02/15 
 Pct Recovery = 88%  Analysis Date = 05/02/15 
 Pct Recovery = 88%  Analysis Date = 04/28/15 
 Pct Recovery = 88%  Analysis Date = 04/28/15 
 Pct Recovery = 88%  Analysis Date = 04/23/15 
 Pct Recovery = 88%  Analysis Date = 04/23/15 
 Pct Recovery = 88%  Analysis Date = 04/19/15 
 Pct Recovery = 88%  Analysis Date = 04/19/15 
 Pct Recovery = 88%  Analysis Date = 04/15/15 
 Pct Recovery = 88%  Analysis Date = 04/15/15 
 Pct Recovery = 88%  Analysis Date = 04/11/15 
 Pct Recovery = 88%  Analysis Date = 04/11/15 
 Pct Recovery = 88%  Analysis Date = 04/07/15 
 Pct Recovery = 88%  Analysis Date = 04/07/15 
 Pct Recovery = 88%  Analysis Date = 04/03/15 
 Pct Recovery = 88%  Analysis Date = 04/03/15 
 Pct Recovery = 88%  Analysis Date = 03/30/15 
 Pct Recovery = 88%  Analysis Date = 03/30/15 
 Pct Recovery = 88%  Analysis Date = 03/25/15 
 Pct Recovery = 89%  Analysis Date = 03/25/15 
 Pct Recovery = 89%  Analysis Date = 03/21/15 
 Pct Recovery = 89%  Analysis Date = 03/21/15 
 Pct Recovery = 89%  Analysis Date = 03/17/15 
 Pct Recovery = 89%  Analysis Date = 03/17/15 
 Pct Recovery = 89%  Analysis Date = 03/13/15 
 Pct Recovery = 89%  Analysis Date = 03/13/15 
 Pct Recovery = 89%  Analysis Date = 03/09/15 
 Pct Recovery = 89%  Analysis Date = 03/09/15 
 Pct Recovery = 89%  Analysis Date = 03/05/15 
 Pct Recovery = 89%  Analysis Date = 03/05/15 
 Pct Recovery = 89%  Analysis Date = 03/01/15 
 Pct Recovery = 89%  Analysis Date = 03/01/15 
 Pct Recovery = 89%  Analysis Date = 02/24/15 
 Pct Recovery = 89%  Analysis Date = 02/24/15 
 Pct Recovery = 89%  Analysis Date = 02/20/15 
 Pct Recovery = 89%  Analysis Date = 02/20/15 
 Pct Recovery = 89%  Analysis Date = 02/16/15 
 Pct Recovery = 89%  Analysis Date = 02/16/15 
 Pct Recovery = 89%  Analysis Date = 02/12/15 
 Pct Recovery = 89%  Analysis Date = 02/12/15 
 Pct Recovery = 89%  Analysis Date = 02/08/15 
 Pct Recovery = 89%  Analysis Date = 02/08/15 
 Pct Recovery = 89%  Analysis Date = 02/04/15 
 Pct Recovery = 89%  Analysis Date = 02/04/15 
 Pct Recovery = 89%  Analysis Date = 01/31/15 
 Pct Recovery = 89%  Analysis Date = 01/31/15 
 Pct Recovery = 89%  Analysis Date = 01/26/15 
 Pct Recovery = 89%  Analysis Date = 01/26/15 
 Pct Recovery = 89%  Analysis Date = 01/22/15 
 Pct Recovery = 89%  Analysis Date = 01/22/15 
 Pct Recovery = 89%  Analysis Date = 01/18/15 
 Pct Recovery = 89%  Analysis Date = 01/18/15 
 Pct Recovery = 89%  Analysis Date = 01/14/15 
 Pct Recovery = 89%  Analysis Date = 01/14/15 
 Pct Recovery = 89%  Analysis Date = 01/10/15 
 Pct Recovery = 89%  Analysis Date = 01/10/15 
 Pct Recovery = 89%  Analysis Date = 01/06/15 
 Pct Recovery = 90%  Analysis Date = 01/06/15 
 Pct Recovery = 90%  Analysis Date = 01/02/15 
 Pct Recovery = 90%  Analysis Date = 01/02/15 
 Pct Recovery = 90%  Analysis Date = 12/28/14 
 Pct Recovery = 90%  Analysis Date = 12/28/14 
 Pct Recovery = 90%  Analysis Date = 12/24/14 
 Pct Recovery = 90%  Analysis Date = 12/24/14 
 Pct Recovery = 90%  Analysis Date = 12/20/14 
 Pct Recovery = 90%  Analysis Date = 12/20/14 
 Pct Recovery = 90%  Analysis Date = 12/16/14 
 Pct Recovery = 90%  Analysis Date = 12/16/14 
 Pct Recovery = 90%  Analysis Date = 12/12/14 
 Pct Recovery = 90%  Analysis Date = 12/12/14 
 Pct Recovery = 90%  Analysis Date = 12/08/14 
 Pct Recovery = 90%  Analysis Date = 12/08/14 
 Pct Recovery = 90%  Analysis Date = 12/04/14 
 Pct Recovery = 90%  Analysis Date = 12/04/14 
 Pct Recovery = 90%  Analysis Date = 11/29/14 
 Pct Recovery = 90%  Analysis Date = 11/29/14 
 Pct Recovery = 90%  Analysis Date = 11/25/14 
 Pct Recovery = 90%  Analysis Date = 11/25/14 
 Pct Recovery = 90%  Analysis Date = 11/21/14 
 Pct Recovery = 90%  Analysis Date = 11/21/14 
 Pct Recovery = 90%  Analysis Date = 11/17/14 
 Pct Recovery = 90%  Analysis Date = 11/17/14 
 Pct Recovery = 90%  Analysis Date = 11/13/14 
 Pct Recovery = 90%  Analysis Date = 11/13/14 
 Pct Recovery = 90%  Analysis Date = 11/09/14 
 Pct Recovery = 90%  Analysis Date = 11/09/14 
 Pct Recovery = 90%  Analysis Date = 11/05/14 
 Pct Recovery = 90%  Analysis Date = 11/05/14 
 Pct Recovery = 90%  Analysis Date = 11/01/14 
 Pct Recovery = 90%  Analysis Date = 11/01/14 
 Pct Recovery = 90%  Analysis Date = 10/27/14 
 Pct Recovery = 90%  Analysis Date = 10/27/14 
 Pct Recovery = 90%  Analysis Date = 10/23/14 
 Pct Recovery = 90%  Analysis Date = 10/23/14 
 Pct Recovery = 90%  Analysis Date = 10/19/14 
 Pct Recovery = 90%  Analysis Date = 10/19/14 
 Pct Recovery = 90%  Analysis Date = 10/15/14 
 Pct Recovery = 90%  Analysis Date = 10/15/14 
 Pct Recovery = 90%  Analysis Date = 10/11/14 
 Pct Recovery = 90%  Analysis Date = 10/11/14 
 Pct Recovery = 90%  Analysis Date = 10/07/14 
 Pct Recovery = 90%  Analysis Date = 10/07/14 
 Pct Recovery = 90%  Analysis Date = 10/03/14 
 Pct Recovery = 90%  Analysis Date = 10/03/14 
 Pct Recovery = 90%  Analysis Date = 09/28/14 
 Pct Recovery = 90%  Analysis Date = 09/28/14 
 Pct Recovery = 90%  Analysis Date = 09/24/14 
 Pct Recovery = 90%  Analysis Date = 09/24/14 
 Pct Recovery = 90%  Analysis Date = 09/20/14 
 Pct Recovery = 90%  Analysis Date = 09/20/14 
 Pct Recovery = 90%  Analysis Date = 09/16/14 
 Pct Recovery = 90%  Analysis Date = 09/16/14 
 Pct Recovery = 90%  Analysis Date = 09/12/14 
 Pct Recovery = 90%  Analysis Date = 09/12/14 
 Pct Recovery = 90%  Analysis Date = 09/08/14 
 Pct Recovery = 90%  Analysis Date = 09/08/14 
 Pct Recovery = 90%  Analysis Date = 09/04/14 
 Pct Recovery = 90%  Analysis Date = 09/04/14 
 Pct Recovery = 90%  Analysis Date = 08/30/14 
 Pct Recovery = 90%  Analysis Date = 08/30/14 
 Pct Recovery = 90%  Analysis Date = 08/26/14 
 Pct Recovery = 90%  Analysis Date = 08/26/14 
 Pct Recovery = 90%  Analysis Date = 08/22/14 
 Pct Recovery = 90%  Analysis Date = 08/22/14 
 Pct Recovery = 90%  Analysis Date = 08/18/14 
 Pct Recovery = 90%  Analysis Date = 08/18/14 
 Pct Recovery = 90%  Analysis Date = 08/14/14 
 Pct Recovery = 90%  Analysis Date = 08/14/14 
 Pct Recovery = 90%  Analysis Date = 08/10/14 
 Pct Recovery = 90%  Analysis Date = 08/10/14 
 Pct Recovery = 90%  Analysis Date = 08/06/14 
 Pct Recovery = 90%  Analysis Date = 08/06/14 
 Pct Recovery = 90%  Analysis Date = 08/01/14 
 Pct Recovery = 90%  Analysis Date = 08/01/14 
 Pct Recovery = 90%  Analysis Date = 07/28/14 
 Pct Recovery = 90%  Analysis Date = 07/28/14 
 Pct Recovery = 90%  Analysis Date = 07/24/14 
 Pct Recovery = 90%  Analysis Date = 07/24/14 
 Pct Recovery = 90%  Analysis Date = 07/20/14 
 Pct Recovery = 90%  Analysis Date = 07/20/14 
 Pct Recovery = 90%  Analysis Date = 07/16/14 
 Pct Recovery = 90%  Analysis Date = 07/16/14 
 Pct Recovery = 90%  Analysis Date = 07/12/14 
 Pct Recovery = 90%  Analysis Date = 07/12/14 
 Pct Recovery = 90%  Analysis Date = 07/08/14 
 Pct Recovery = 90%  Analysis Date = 07/08/14 
 Pct Recovery = 90%  Analysis Date = 07/03/14 
 Pct Recovery = 90%  Analysis Date = 07/03/14 
 Pct Recovery = 90%  Analysis Date = 06/29/14 
 Pct Recovery = 90%  Analysis Date = 06/29/14 
 Pct Recovery = 90%  Analysis Date = 06/25/14 
 Pct Recovery = 90%  Analysis Date = 06/25/14 
 Pct Recovery = 90%  Analysis Date = 06/21/14 
 Pct Recovery = 90%  Analysis Date = 06/21/14 
 Pct Recovery = 90%  Analysis Date = 06/17/14 
 Pct Recovery = 90%  Analysis Date = 06/17/14 
 Pct Recovery = 90%  Analysis Date = 06/13/14 
 Pct Recovery = 90%  Analysis Date = 06/13/14 
 Pct Recovery = 90%  Analysis Date = 06/09/14 
 Pct Recovery = 90%  Analysis Date = 06/09/14 
 Pct Recovery = 90%  Analysis Date = 06/04/14 
 Pct Recovery = 91%  Analysis Date = 06/04/14 
 Pct Recovery = 91%  Analysis Date = 05/31/14 
 Pct Recovery = 91%  Analysis Date = 05/31/14 
 Pct Recovery = 91%  Analysis Date = 05/27/14 
 Pct Recovery = 91%  Analysis Date = 05/27/14 
 Pct Recovery = 91%  Analysis Date = 05/23/14 
 Pct Recovery = 91%  Analysis Date = 05/23/14 
 Pct Recovery = 91%  Analysis Date = 05/19/14 
 Pct Recovery = 91%  Analysis Date = 05/19/14 
 Pct Recovery = 91%  Analysis Date = 05/15/14 
 Pct Recovery = 91%  Analysis Date = 05/15/14 
 Pct Recovery = 91%  Analysis Date = 05/11/14 
 Pct Recovery = 91%  Analysis Date = 05/11/14 
 Pct Recovery = 91%  Analysis Date = 05/07/14 
 Pct Recovery = 91%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
1-OCTANOL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 39 86% 8% 85% 9%
Total 39 86% 8% 85% 9%

Sample Statistics
1-OCTANOL

Characteristic N % % Basis
Plotted 39 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 39 .  
False Negatives 0 0% 0 out of 39
Not Spiked 16 .  
False Positives 0 0% 0 out of 16

BQS OBSP Determination:
1METHOXY-4(2-PROPENYL)BENZENE
METHOD: 4437 , TESTIDCODE: 68066GM016
Open Data Set

 Analysis Date = 03/19/15 
 SpikeMix = Supelco LC06437: 20 µl & NSI 031814: 20 µl 
 Pct Recovery = 96%  Analysis Date = 01/10/15 
 SpikeMix = Abs 032014: 20 µl & ERA 0321-14-05A: 20 µl 
 Pct Recovery = 79%  Analysis Date = 08/20/14 
 SpikeMix = Supelco LC06437: 20 µl & Abs 032014: 20 µl 
 Pct Recovery = 143%  Analysis Date = 07/23/14 
 SpikeMix = Accu 214031128: 20 µl & Abs 032014: 20 µl 
 Pct Recovery = 113%  Analysis Date = 07/03/14 
 SpikeMix = Abs 032014: 20 µl & ChemService 2615700: 20 µl 
 Pct Recovery = 120%  Analysis Date = 06/06/14 
 SpikeMix = NSI 031814: 20 µl & ChemService 2615700: 20 µl 
 Pct Recovery = 117%  Analysis Date = 05/07/14 
 SpikeMix = NSI 031814: 20 µl & Accu 214031128: 20 µl 
 Pct Recovery = 85%  Analysis Date = 06/29/16 
 SpikeMix = NSI 041516: 40 µl & ChemService 5082800: 40 µl 
 Pct Recovery = 81%  Analysis Date = 08/11/16 
 SpikeMix = Phenova B20160303: 25 µl & Supelco LC20145V: 25 µl & NSI 041416HVOC: 25 µl 
 Pct Recovery = 77%  Analysis Date = 07/14/16 
 SpikeMix = NSI 041516: 25 µl & ChemService 5082800: 25 µl & NSI 041416HVOC: 25 µl 
 Pct Recovery = 89%  Analysis Date = 04/25/15 
 SpikeMix = Abs 032014: 10 µl & ERA 0321-14-05A: 10 µl 
 Pct Recovery = 92%  Analysis Date = 12/13/14 
 SpikeMix = Accu 214031128: 10 µl & NSI 031814: 10 µl 
 Pct Recovery = 83%  Analysis Date = 09/11/14 
 SpikeMix = Accu 214031128: 10 µl & Abs 032014: 10 µl 
 Pct Recovery = 75%  Analysis Date = 07/30/14 
 SpikeMix = NSI 031814: 10 µl & ChemService 2615700: 10 µl 
 Pct Recovery = 108%  Analysis Date = 06/17/14 
 SpikeMix = Supelco LC06437: 10 µl & Abs 032014: 10 µl 
 Pct Recovery = 119%  Analysis Date = 10/09/15 
 SpikeMix = ERA 0601-15-05: 25 µl & Accu 215041338: 25 µl 
 Pct Recovery = 79%  Analysis Date = 10/09/15 
 SpikeMix = Supelco LC13544: 25 µl & NSI 050515HVOC: 25 µl 
 Pct Recovery = 87%  Analysis Date = 06/26/15 
 SpikeMix = ChemService 3818700: 25 µl & Accu 215041338: 25 µl 
 Pct Recovery = 71%  Analysis Date = 07/27/16 
 SpikeMix = ChemService 5082800: 15 µl & Supelco LC20145V: 15 µl & Accu 216041225: 15 µl 
 Pct Recovery = 69%  Analysis Date = 07/06/16 
 SpikeMix = Phenova B20160303: 15 µl & Accu 216041354: 15 µl & NSI 041416HVOC: 15 µl 
 Pct Recovery = 74%  Analysis Date = 06/23/16 
 SpikeMix = . 
 Pct Recovery = 83%  Analysis Date = 06/03/16 
 SpikeMix = NSI 041516: 15 µl & Phenova B20160303: 15 µl & NSI 041416HVOC: 15 µl 
 Pct Recovery = 91%  Analysis Date = 04/28/16 
 SpikeMix = ChemService 3818700: 15 µl & Supelco LC13544: 15 µl 
 Pct Recovery = 93%  Analysis Date = 11/25/15 
 SpikeMix = Accu 215041338: 15 µl & Abs 040315: 15 µl 
 Pct Recovery = 72%  Analysis Date = 09/05/15 
 SpikeMix = Accu 215041338: 15 µl & NSI 050515HVOC: 15 µl 
 Pct Recovery = 67%  Analysis Date = 08/24/15 
 SpikeMix = ERA 0601-15-05: 15 µl & Supelco LC13544: 15 µl 
 Pct Recovery = 70%  Analysis Date = 07/30/15 
 SpikeMix = Supelco LC13544: 15 µl & NSI 050515HVOC: 15 µl 
 Pct Recovery = 78%  Analysis Date = 05/14/15 
 SpikeMix = ChemService 3818700: 15 µl & Supelco LC13544: 15 µl 
 Pct Recovery = 101%  Analysis Date = 03/22/16 
 SpikeMix = Supelco LC13544: 10 µl & NSI 050515HVOC: 10 µl 
 Pct Recovery = 85%  Analysis Date = 02/12/16 
 SpikeMix = ERA 0601-15-05: 10 µl & Accu 215041338: 10 µl 
 Pct Recovery = 73%  Analysis Date = 01/05/16 
 SpikeMix = Accu 215041338: 10 µl & Abs 040315: 10 µl 
 Pct Recovery = 91%  Analysis Date = 12/10/15 
 SpikeMix = ChemService 3818700: 10 µl & Supelco LC13544: 10 µl 
 Pct Recovery = 84%  Analysis Date = 05/20/15 
 SpikeMix = ChemService 3818700: 10 µl & Accu 215041338: 10 µl 
 Pct Recovery = 115%  Analysis Date = 05/05/15 
 SpikeMix = Supelco LC13544: 10 µl & Abs 040315: 10 µl 
 Pct Recovery = 98%  Analysis Date = 08/10/16 
 Pct Recovery = 82%  Analysis Date = 08/06/16 
 Pct Recovery = 82%  Analysis Date = 08/06/16 
 Pct Recovery = 82%  Analysis Date = 08/02/16 
 Pct Recovery = 82%  Analysis Date = 08/02/16 
 Pct Recovery = 82%  Analysis Date = 07/29/16 
 Pct Recovery = 82%  Analysis Date = 07/29/16 
 Pct Recovery = 82%  Analysis Date = 07/25/16 
 Pct Recovery = 82%  Analysis Date = 07/25/16 
 Pct Recovery = 82%  Analysis Date = 07/21/16 
 Pct Recovery = 82%  Analysis Date = 07/21/16 
 Pct Recovery = 82%  Analysis Date = 07/17/16 
 Pct Recovery = 82%  Analysis Date = 07/17/16 
 Pct Recovery = 82%  Analysis Date = 07/13/16 
 Pct Recovery = 82%  Analysis Date = 07/13/16 
 Pct Recovery = 82%  Analysis Date = 07/08/16 
 Pct Recovery = 82%  Analysis Date = 07/08/16 
 Pct Recovery = 82%  Analysis Date = 07/04/16 
 Pct Recovery = 82%  Analysis Date = 07/04/16 
 Pct Recovery = 82%  Analysis Date = 06/30/16 
 Pct Recovery = 82%  Analysis Date = 06/30/16 
 Pct Recovery = 82%  Analysis Date = 06/26/16 
 Pct Recovery = 82%  Analysis Date = 06/26/16 
 Pct Recovery = 82%  Analysis Date = 06/22/16 
 Pct Recovery = 82%  Analysis Date = 06/22/16 
 Pct Recovery = 82%  Analysis Date = 06/18/16 
 Pct Recovery = 82%  Analysis Date = 06/18/16 
 Pct Recovery = 82%  Analysis Date = 06/14/16 
 Pct Recovery = 82%  Analysis Date = 06/14/16 
 Pct Recovery = 82%  Analysis Date = 06/09/16 
 Pct Recovery = 82%  Analysis Date = 06/09/16 
 Pct Recovery = 82%  Analysis Date = 06/05/16 
 Pct Recovery = 82%  Analysis Date = 06/05/16 
 Pct Recovery = 82%  Analysis Date = 06/01/16 
 Pct Recovery = 82%  Analysis Date = 06/01/16 
 Pct Recovery = 82%  Analysis Date = 05/28/16 
 Pct Recovery = 82%  Analysis Date = 05/28/16 
 Pct Recovery = 82%  Analysis Date = 05/24/16 
 Pct Recovery = 82%  Analysis Date = 05/24/16 
 Pct Recovery = 82%  Analysis Date = 05/20/16 
 Pct Recovery = 82%  Analysis Date = 05/20/16 
 Pct Recovery = 82%  Analysis Date = 05/16/16 
 Pct Recovery = 82%  Analysis Date = 05/16/16 
 Pct Recovery = 82%  Analysis Date = 05/12/16 
 Pct Recovery = 82%  Analysis Date = 05/12/16 
 Pct Recovery = 82%  Analysis Date = 05/07/16 
 Pct Recovery = 82%  Analysis Date = 05/07/16 
 Pct Recovery = 82%  Analysis Date = 05/03/16 
 Pct Recovery = 82%  Analysis Date = 05/03/16 
 Pct Recovery = 82%  Analysis Date = 04/29/16 
 Pct Recovery = 82%  Analysis Date = 04/29/16 
 Pct Recovery = 82%  Analysis Date = 04/25/16 
 Pct Recovery = 82%  Analysis Date = 04/25/16 
 Pct Recovery = 82%  Analysis Date = 04/21/16 
 Pct Recovery = 81%  Analysis Date = 04/21/16 
 Pct Recovery = 81%  Analysis Date = 04/17/16 
 Pct Recovery = 81%  Analysis Date = 04/17/16 
 Pct Recovery = 81%  Analysis Date = 04/13/16 
 Pct Recovery = 81%  Analysis Date = 04/13/16 
 Pct Recovery = 81%  Analysis Date = 04/08/16 
 Pct Recovery = 81%  Analysis Date = 04/08/16 
 Pct Recovery = 81%  Analysis Date = 04/04/16 
 Pct Recovery = 81%  Analysis Date = 04/04/16 
 Pct Recovery = 81%  Analysis Date = 03/31/16 
 Pct Recovery = 81%  Analysis Date = 03/31/16 
 Pct Recovery = 81%  Analysis Date = 03/27/16 
 Pct Recovery = 81%  Analysis Date = 03/27/16 
 Pct Recovery = 81%  Analysis Date = 03/23/16 
 Pct Recovery = 81%  Analysis Date = 03/23/16 
 Pct Recovery = 81%  Analysis Date = 03/19/16 
 Pct Recovery = 81%  Analysis Date = 03/19/16 
 Pct Recovery = 81%  Analysis Date = 03/15/16 
 Pct Recovery = 81%  Analysis Date = 03/15/16 
 Pct Recovery = 81%  Analysis Date = 03/11/16 
 Pct Recovery = 81%  Analysis Date = 03/11/16 
 Pct Recovery = 81%  Analysis Date = 03/06/16 
 Pct Recovery = 81%  Analysis Date = 03/06/16 
 Pct Recovery = 81%  Analysis Date = 03/02/16 
 Pct Recovery = 81%  Analysis Date = 03/02/16 
 Pct Recovery = 81%  Analysis Date = 02/27/16 
 Pct Recovery = 81%  Analysis Date = 02/27/16 
 Pct Recovery = 81%  Analysis Date = 02/23/16 
 Pct Recovery = 81%  Analysis Date = 02/23/16 
 Pct Recovery = 81%  Analysis Date = 02/19/16 
 Pct Recovery = 81%  Analysis Date = 02/19/16 
 Pct Recovery = 81%  Analysis Date = 02/15/16 
 Pct Recovery = 81%  Analysis Date = 02/15/16 
 Pct Recovery = 81%  Analysis Date = 02/11/16 
 Pct Recovery = 81%  Analysis Date = 02/11/16 
 Pct Recovery = 81%  Analysis Date = 02/06/16 
 Pct Recovery = 81%  Analysis Date = 02/06/16 
 Pct Recovery = 81%  Analysis Date = 02/02/16 
 Pct Recovery = 81%  Analysis Date = 02/02/16 
 Pct Recovery = 81%  Analysis Date = 01/29/16 
 Pct Recovery = 81%  Analysis Date = 01/29/16 
 Pct Recovery = 81%  Analysis Date = 01/25/16 
 Pct Recovery = 81%  Analysis Date = 01/25/16 
 Pct Recovery = 81%  Analysis Date = 01/21/16 
 Pct Recovery = 81%  Analysis Date = 01/21/16 
 Pct Recovery = 81%  Analysis Date = 01/17/16 
 Pct Recovery = 81%  Analysis Date = 01/17/16 
 Pct Recovery = 81%  Analysis Date = 01/13/16 
 Pct Recovery = 81%  Analysis Date = 01/13/16 
 Pct Recovery = 81%  Analysis Date = 01/08/16 
 Pct Recovery = 81%  Analysis Date = 01/08/16 
 Pct Recovery = 81%  Analysis Date = 01/04/16 
 Pct Recovery = 80%  Analysis Date = 01/04/16 
 Pct Recovery = 80%  Analysis Date = 12/31/15 
 Pct Recovery = 80%  Analysis Date = 12/31/15 
 Pct Recovery = 80%  Analysis Date = 12/27/15 
 Pct Recovery = 80%  Analysis Date = 12/27/15 
 Pct Recovery = 80%  Analysis Date = 12/23/15 
 Pct Recovery = 80%  Analysis Date = 12/23/15 
 Pct Recovery = 80%  Analysis Date = 12/19/15 
 Pct Recovery = 80%  Analysis Date = 12/19/15 
 Pct Recovery = 80%  Analysis Date = 12/15/15 
 Pct Recovery = 80%  Analysis Date = 12/15/15 
 Pct Recovery = 80%  Analysis Date = 12/11/15 
 Pct Recovery = 80%  Analysis Date = 12/11/15 
 Pct Recovery = 80%  Analysis Date = 12/06/15 
 Pct Recovery = 80%  Analysis Date = 12/06/15 
 Pct Recovery = 80%  Analysis Date = 12/02/15 
 Pct Recovery = 80%  Analysis Date = 12/02/15 
 Pct Recovery = 80%  Analysis Date = 11/28/15 
 Pct Recovery = 80%  Analysis Date = 11/28/15 
 Pct Recovery = 80%  Analysis Date = 11/24/15 
 Pct Recovery = 80%  Analysis Date = 11/24/15 
 Pct Recovery = 80%  Analysis Date = 11/20/15 
 Pct Recovery = 80%  Analysis Date = 11/20/15 
 Pct Recovery = 80%  Analysis Date = 11/16/15 
 Pct Recovery = 80%  Analysis Date = 11/16/15 
 Pct Recovery = 80%  Analysis Date = 11/12/15 
 Pct Recovery = 81%  Analysis Date = 11/12/15 
 Pct Recovery = 81%  Analysis Date = 11/07/15 
 Pct Recovery = 81%  Analysis Date = 11/07/15 
 Pct Recovery = 81%  Analysis Date = 11/03/15 
 Pct Recovery = 81%  Analysis Date = 11/03/15 
 Pct Recovery = 81%  Analysis Date = 10/30/15 
 Pct Recovery = 81%  Analysis Date = 10/30/15 
 Pct Recovery = 81%  Analysis Date = 10/26/15 
 Pct Recovery = 81%  Analysis Date = 10/26/15 
 Pct Recovery = 81%  Analysis Date = 10/22/15 
 Pct Recovery = 81%  Analysis Date = 10/22/15 
 Pct Recovery = 81%  Analysis Date = 10/18/15 
 Pct Recovery = 81%  Analysis Date = 10/18/15 
 Pct Recovery = 81%  Analysis Date = 10/14/15 
 Pct Recovery = 82%  Analysis Date = 10/14/15 
 Pct Recovery = 82%  Analysis Date = 10/10/15 
 Pct Recovery = 82%  Analysis Date = 10/10/15 
 Pct Recovery = 82%  Analysis Date = 10/05/15 
 Pct Recovery = 82%  Analysis Date = 10/05/15 
 Pct Recovery = 82%  Analysis Date = 10/01/15 
 Pct Recovery = 82%  Analysis Date = 10/01/15 
 Pct Recovery = 82%  Analysis Date = 09/27/15 
 Pct Recovery = 82%  Analysis Date = 09/27/15 
 Pct Recovery = 82%  Analysis Date = 09/23/15 
 Pct Recovery = 83%  Analysis Date = 09/23/15 
 Pct Recovery = 83%  Analysis Date = 09/19/15 
 Pct Recovery = 83%  Analysis Date = 09/19/15 
 Pct Recovery = 83%  Analysis Date = 09/15/15 
 Pct Recovery = 83%  Analysis Date = 09/15/15 
 Pct Recovery = 83%  Analysis Date = 09/11/15 
 Pct Recovery = 83%  Analysis Date = 09/11/15 
 Pct Recovery = 83%  Analysis Date = 09/06/15 
 Pct Recovery = 83%  Analysis Date = 09/06/15 
 Pct Recovery = 83%  Analysis Date = 09/02/15 
 Pct Recovery = 84%  Analysis Date = 09/02/15 
 Pct Recovery = 84%  Analysis Date = 08/29/15 
 Pct Recovery = 84%  Analysis Date = 08/29/15 
 Pct Recovery = 84%  Analysis Date = 08/25/15 
 Pct Recovery = 84%  Analysis Date = 08/25/15 
 Pct Recovery = 84%  Analysis Date = 08/21/15 
 Pct Recovery = 84%  Analysis Date = 08/21/15 
 Pct Recovery = 84%  Analysis Date = 08/17/15 
 Pct Recovery = 84%  Analysis Date = 08/17/15 
 Pct Recovery = 84%  Analysis Date = 08/13/15 
 Pct Recovery = 85%  Analysis Date = 08/13/15 
 Pct Recovery = 85%  Analysis Date = 08/08/15 
 Pct Recovery = 85%  Analysis Date = 08/08/15 
 Pct Recovery = 85%  Analysis Date = 08/04/15 
 Pct Recovery = 85%  Analysis Date = 08/04/15 
 Pct Recovery = 85%  Analysis Date = 07/31/15 
 Pct Recovery = 85%  Analysis Date = 07/31/15 
 Pct Recovery = 85%  Analysis Date = 07/27/15 
 Pct Recovery = 85%  Analysis Date = 07/27/15 
 Pct Recovery = 85%  Analysis Date = 07/23/15 
 Pct Recovery = 85%  Analysis Date = 07/23/15 
 Pct Recovery = 85%  Analysis Date = 07/19/15 
 Pct Recovery = 86%  Analysis Date = 07/19/15 
 Pct Recovery = 86%  Analysis Date = 07/15/15 
 Pct Recovery = 86%  Analysis Date = 07/15/15 
 Pct Recovery = 86%  Analysis Date = 07/11/15 
 Pct Recovery = 86%  Analysis Date = 07/11/15 
 Pct Recovery = 86%  Analysis Date = 07/06/15 
 Pct Recovery = 86%  Analysis Date = 07/06/15 
 Pct Recovery = 86%  Analysis Date = 07/02/15 
 Pct Recovery = 86%  Analysis Date = 07/02/15 
 Pct Recovery = 86%  Analysis Date = 06/28/15 
 Pct Recovery = 86%  Analysis Date = 06/28/15 
 Pct Recovery = 86%  Analysis Date = 06/24/15 
 Pct Recovery = 86%  Analysis Date = 06/24/15 
 Pct Recovery = 86%  Analysis Date = 06/20/15 
 Pct Recovery = 87%  Analysis Date = 06/20/15 
 Pct Recovery = 87%  Analysis Date = 06/16/15 
 Pct Recovery = 87%  Analysis Date = 06/16/15 
 Pct Recovery = 87%  Analysis Date = 06/12/15 
 Pct Recovery = 87%  Analysis Date = 06/12/15 
 Pct Recovery = 87%  Analysis Date = 06/07/15 
 Pct Recovery = 87%  Analysis Date = 06/07/15 
 Pct Recovery = 87%  Analysis Date = 06/03/15 
 Pct Recovery = 87%  Analysis Date = 06/03/15 
 Pct Recovery = 87%  Analysis Date = 05/30/15 
 Pct Recovery = 87%  Analysis Date = 05/30/15 
 Pct Recovery = 87%  Analysis Date = 05/26/15 
 Pct Recovery = 87%  Analysis Date = 05/26/15 
 Pct Recovery = 87%  Analysis Date = 05/22/15 
 Pct Recovery = 88%  Analysis Date = 05/22/15 
 Pct Recovery = 88%  Analysis Date = 05/18/15 
 Pct Recovery = 88%  Analysis Date = 05/18/15 
 Pct Recovery = 88%  Analysis Date = 05/14/15 
 Pct Recovery = 88%  Analysis Date = 05/14/15 
 Pct Recovery = 88%  Analysis Date = 05/10/15 
 Pct Recovery = 88%  Analysis Date = 05/10/15 
 Pct Recovery = 88%  Analysis Date = 05/05/15 
 Pct Recovery = 88%  Analysis Date = 05/05/15 
 Pct Recovery = 88%  Analysis Date = 05/01/15 
 Pct Recovery = 88%  Analysis Date = 05/01/15 
 Pct Recovery = 88%  Analysis Date = 04/27/15 
 Pct Recovery = 89%  Analysis Date = 04/27/15 
 Pct Recovery = 89%  Analysis Date = 04/23/15 
 Pct Recovery = 89%  Analysis Date = 04/23/15 
 Pct Recovery = 89%  Analysis Date = 04/19/15 
 Pct Recovery = 89%  Analysis Date = 04/19/15 
 Pct Recovery = 89%  Analysis Date = 04/15/15 
 Pct Recovery = 90%  Analysis Date = 04/15/15 
 Pct Recovery = 90%  Analysis Date = 04/11/15 
 Pct Recovery = 90%  Analysis Date = 04/11/15 
 Pct Recovery = 90%  Analysis Date = 04/06/15 
 Pct Recovery = 90%  Analysis Date = 04/06/15 
 Pct Recovery = 90%  Analysis Date = 04/02/15 
 Pct Recovery = 91%  Analysis Date = 04/02/15 
 Pct Recovery = 91%  Analysis Date = 03/29/15 
 Pct Recovery = 91%  Analysis Date = 03/29/15 
 Pct Recovery = 91%  Analysis Date = 03/25/15 
 Pct Recovery = 91%  Analysis Date = 03/25/15 
 Pct Recovery = 91%  Analysis Date = 03/21/15 
 Pct Recovery = 92%  Analysis Date = 03/21/15 
 Pct Recovery = 92%  Analysis Date = 03/17/15 
 Pct Recovery = 92%  Analysis Date = 03/17/15 
 Pct Recovery = 92%  Analysis Date = 03/13/15 
 Pct Recovery = 92%  Analysis Date = 03/13/15 
 Pct Recovery = 92%  Analysis Date = 03/08/15 
 Pct Recovery = 93%  Analysis Date = 03/08/15 
 Pct Recovery = 93%  Analysis Date = 03/04/15 
 Pct Recovery = 93%  Analysis Date = 03/04/15 
 Pct Recovery = 93%  Analysis Date = 02/28/15 
 Pct Recovery = 93%  Analysis Date = 02/28/15 
 Pct Recovery = 93%  Analysis Date = 02/24/15 
 Pct Recovery = 94%  Analysis Date = 02/24/15 
 Pct Recovery = 94%  Analysis Date = 02/20/15 
 Pct Recovery = 94%  Analysis Date = 02/20/15 
 Pct Recovery = 94%  Analysis Date = 02/16/15 
 Pct Recovery = 94%  Analysis Date = 02/16/15 
 Pct Recovery = 94%  Analysis Date = 02/12/15 
 Pct Recovery = 95%  Analysis Date = 02/12/15 
 Pct Recovery = 95%  Analysis Date = 02/08/15 
 Pct Recovery = 95%  Analysis Date = 02/08/15 
 Pct Recovery = 95%  Analysis Date = 02/03/15 
 Pct Recovery = 95%  Analysis Date = 02/03/15 
 Pct Recovery = 95%  Analysis Date = 01/30/15 
 Pct Recovery = 96%  Analysis Date = 01/30/15 
 Pct Recovery = 96%  Analysis Date = 01/26/15 
 Pct Recovery = 96%  Analysis Date = 01/26/15 
 Pct Recovery = 96%  Analysis Date = 01/22/15 
 Pct Recovery = 96%  Analysis Date = 01/22/15 
 Pct Recovery = 96%  Analysis Date = 01/18/15 
 Pct Recovery = 97%  Analysis Date = 01/18/15 
 Pct Recovery = 97%  Analysis Date = 01/14/15 
 Pct Recovery = 97%  Analysis Date = 01/14/15 
 Pct Recovery = 97%  Analysis Date = 01/10/15 
 Pct Recovery = 97%  Analysis Date = 01/10/15 
 Pct Recovery = 97%  Analysis Date = 01/05/15 
 Pct Recovery = 98%  Analysis Date = 01/05/15 
 Pct Recovery = 98%  Analysis Date = 01/01/15 
 Pct Recovery = 98%  Analysis Date = 01/01/15 
 Pct Recovery = 98%  Analysis Date = 12/28/14 
 Pct Recovery = 98%  Analysis Date = 12/28/14 
 Pct Recovery = 98%  Analysis Date = 12/24/14 
 Pct Recovery = 99%  Analysis Date = 12/24/14 
 Pct Recovery = 99%  Analysis Date = 12/20/14 
 Pct Recovery = 99%  Analysis Date = 12/20/14 
 Pct Recovery = 99%  Analysis Date = 12/16/14 
 Pct Recovery = 99%  Analysis Date = 12/16/14 
 Pct Recovery = 99%  Analysis Date = 12/12/14 
 Pct Recovery = 100%  Analysis Date = 12/12/14 
 Pct Recovery = 100%  Analysis Date = 12/08/14 
 Pct Recovery = 100%  Analysis Date = 12/08/14 
 Pct Recovery = 100%  Analysis Date = 12/03/14 
 Pct Recovery = 100%  Analysis Date = 12/03/14 
 Pct Recovery = 100%  Analysis Date = 11/29/14 
 Pct Recovery = 100%  Analysis Date = 11/29/14 
 Pct Recovery = 100%  Analysis Date = 11/25/14 
 Pct Recovery = 100%  Analysis Date = 11/25/14 
 Pct Recovery = 100%  Analysis Date = 11/21/14 
 Pct Recovery = 101%  Analysis Date = 11/21/14 
 Pct Recovery = 101%  Analysis Date = 11/17/14 
 Pct Recovery = 101%  Analysis Date = 11/17/14 
 Pct Recovery = 101%  Analysis Date = 11/13/14 
 Pct Recovery = 101%  Analysis Date = 11/13/14 
 Pct Recovery = 101%  Analysis Date = 11/09/14 
 Pct Recovery = 101%  Analysis Date = 11/09/14 
 Pct Recovery = 101%  Analysis Date = 11/04/14 
 Pct Recovery = 102%  Analysis Date = 11/04/14 
 Pct Recovery = 102%  Analysis Date = 10/31/14 
 Pct Recovery = 102%  Analysis Date = 10/31/14 
 Pct Recovery = 102%  Analysis Date = 10/27/14 
 Pct Recovery = 102%  Analysis Date = 10/27/14 
 Pct Recovery = 102%  Analysis Date = 10/23/14 
 Pct Recovery = 102%  Analysis Date = 10/23/14 
 Pct Recovery = 102%  Analysis Date = 10/19/14 
 Pct Recovery = 103%  Analysis Date = 10/19/14 
 Pct Recovery = 103%  Analysis Date = 10/15/14 
 Pct Recovery = 103%  Analysis Date = 10/15/14 
 Pct Recovery = 103%  Analysis Date = 10/11/14 
 Pct Recovery = 103%  Analysis Date = 10/11/14 
 Pct Recovery = 103%  Analysis Date = 10/06/14 
 Pct Recovery = 103%  Analysis Date = 10/06/14 
 Pct Recovery = 103%  Analysis Date = 10/02/14 
 Pct Recovery = 103%  Analysis Date = 10/02/14 
 Pct Recovery = 103%  Analysis Date = 09/28/14 
 Pct Recovery = 104%  Analysis Date = 09/28/14 
 Pct Recovery = 104%  Analysis Date = 09/24/14 
 Pct Recovery = 104%  Analysis Date = 09/24/14 
 Pct Recovery = 104%  Analysis Date = 09/20/14 
 Pct Recovery = 104%  Analysis Date = 09/20/14 
 Pct Recovery = 104%  Analysis Date = 09/16/14 
 Pct Recovery = 104%  Analysis Date = 09/16/14 
 Pct Recovery = 104%  Analysis Date = 09/12/14 
 Pct Recovery = 105%  Analysis Date = 09/12/14 
 Pct Recovery = 105%  Analysis Date = 09/08/14 
 Pct Recovery = 105%  Analysis Date = 09/08/14 
 Pct Recovery = 105%  Analysis Date = 09/03/14 
 Pct Recovery = 105%  Analysis Date = 09/03/14 
 Pct Recovery = 105%  Analysis Date = 08/30/14 
 Pct Recovery = 105%  Analysis Date = 08/30/14 
 Pct Recovery = 105%  Analysis Date = 08/26/14 
 Pct Recovery = 105%  Analysis Date = 08/26/14 
 Pct Recovery = 105%  Analysis Date = 08/22/14 
 Pct Recovery = 106%  Analysis Date = 08/22/14 
 Pct Recovery = 106%  Analysis Date = 08/18/14 
 Pct Recovery = 106%  Analysis Date = 08/18/14 
 Pct Recovery = 106%  Analysis Date = 08/14/14 
 Pct Recovery = 106%  Analysis Date = 08/14/14 
 Pct Recovery = 106%  Analysis Date = 08/10/14 
 Pct Recovery = 106%  Analysis Date = 08/10/14 
 Pct Recovery = 106%  Analysis Date = 08/05/14 
 Pct Recovery = 107%  Analysis Date = 08/05/14 
 Pct Recovery = 107%  Analysis Date = 08/01/14 
 Pct Recovery = 107%  Analysis Date = 08/01/14 
 Pct Recovery = 107%  Analysis Date = 07/28/14 
 Pct Recovery = 107%  Analysis Date = 07/28/14 
 Pct Recovery = 107%  Analysis Date = 07/24/14 
 Pct Recovery = 107%  Analysis Date = 07/24/14 
 Pct Recovery = 107%  Analysis Date = 07/20/14 
 Pct Recovery = 108%  Analysis Date = 07/20/14 
 Pct Recovery = 108%  Analysis Date = 07/16/14 
 Pct Recovery = 108%  Analysis Date = 07/16/14 
 Pct Recovery = 108%  Analysis Date = 07/12/14 
 Pct Recovery = 108%  Analysis Date = 07/12/14 
 Pct Recovery = 108%  Analysis Date = 07/08/14 
 Pct Recovery = 108%  Analysis Date = 07/08/14 
 Pct Recovery = 108%  Analysis Date = 07/03/14 
 Pct Recovery = 109%  Analysis Date = 07/03/14 
 Pct Recovery = 109%  Analysis Date = 06/29/14 
 Pct Recovery = 109%  Analysis Date = 06/29/14 
 Pct Recovery = 109%  Analysis Date = 06/25/14 
 Pct Recovery = 109%  Analysis Date = 06/25/14 
 Pct Recovery = 109%  Analysis Date = 06/21/14 
 Pct Recovery = 109%  Analysis Date = 06/21/14 
 Pct Recovery = 109%  Analysis Date = 06/17/14 
 Pct Recovery = 110%  Analysis Date = 06/17/14 
 Pct Recovery = 110%  Analysis Date = 06/13/14 
 Pct Recovery = 110%  Analysis Date = 06/13/14 
 Pct Recovery = 110%  Analysis Date = 06/09/14 
 Pct Recovery = 110%  Analysis Date = 06/09/14 
 Pct Recovery = 110%  Analysis Date = 06/04/14 
 Pct Recovery = 110%  Analysis Date = 06/04/14 
 Pct Recovery = 110%  Analysis Date = 05/31/14 
 Pct Recovery = 111%  Analysis Date = 05/31/14 
 Pct Recovery = 111%  Analysis Date = 05/27/14 
 Pct Recovery = 111%  Analysis Date = 05/27/14 
 Pct Recovery = 111%  Analysis Date = 05/23/14 
 Pct Recovery = 111%  Analysis Date = 05/23/14 
 Pct Recovery = 111%  Analysis Date = 05/19/14 
 Pct Recovery = 111%  Analysis Date = 05/19/14 
 Pct Recovery = 111%  Analysis Date = 05/15/14 
 Pct Recovery = 112%  Analysis Date = 05/15/14 
 Pct Recovery = 112%  Analysis Date = 05/11/14 
 Pct Recovery = 112%  Analysis Date = 05/11/14 
 Pct Recovery = 112%  Analysis Date = 05/07/14 
 Pct Recovery = 112%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
1METHOXY-4(2-PROPENYL)BENZENE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 34 90% 18% 85% 15%
Total 34 90% 18% 85% 15%

Sample Statistics
1METHOXY-4(2-PROPENYL)BENZENE

Characteristic N % % Basis
Plotted 34 100% Spiked
Estimated Values 1 3% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 34 .  
False Negatives 0 0% 0 out of 34
Not Spiked 21 .  
False Positives 0 0% 0 out of 21

BQS OBSP Determination:
2-ETHOXYETHYL ACETATE
METHOD: 4437 , TESTIDCODE: 68728GM016
Open Data Set

 Analysis Date = 03/19/15 
 SpikeMix = Supelco LC06437: 20 µl & NSI 031814: 20 µl 
 Pct Recovery = 207%  Analysis Date = 10/09/15 
 SpikeMix = ERA 0601-15-05: 25 µl & Accu 215041338: 25 µl 
 Pct Recovery = 96%  Analysis Date = 06/26/15 
 SpikeMix = ChemService 3818700: 25 µl & Accu 215041338: 25 µl 
 Pct Recovery = 88%  Analysis Date = 10/09/15 
 SpikeMix = Supelco LC13544: 25 µl & NSI 050515HVOC: 25 µl 
 Pct Recovery = 111%  Analysis Date = 08/13/14 
 SpikeMix = ERA 0321-14-05: 20 µl & Accu 214031128: 20 µl 
 Pct Recovery = 139%  Analysis Date = 07/23/14 
 SpikeMix = Accu 214031128: 20 µl & Abs 032014: 20 µl 
 Pct Recovery = 135%  Analysis Date = 07/11/14 
 SpikeMix = ChemService 2615700: 20 µl & Accu 214031128: 20 µl 
 Pct Recovery = 154%  Analysis Date = 05/07/14 
 SpikeMix = NSI 031814: 20 µl & Accu 214031128: 20 µl 
 Pct Recovery = 113%  Analysis Date = 08/20/14 
 SpikeMix = Supelco LC06437: 20 µl & Abs 032014: 20 µl 
 Pct Recovery = 173%  Analysis Date = 06/07/14 
 SpikeMix = ChemService 2615700: 20 µl & Supelco LC06437: 20 µl 
 Pct Recovery = 129%  Analysis Date = 07/27/16 
 SpikeMix = ChemService 5082800: 15 µl & Supelco LC20145V: 15 µl & Accu 216041225: 15 µl 
 Pct Recovery = 84%  Analysis Date = 05/20/16 
 SpikeMix = Accu 216041354: 15 µl & NSI 041516: 15 µl & Accu 216041225: 15 µl 
 Pct Recovery = 95%  Analysis Date = 11/25/15 
 SpikeMix = Accu 215041338: 15 µl & Abs 040315: 15 µl 
 Pct Recovery = 97%  Analysis Date = 09/05/15 
 SpikeMix = Accu 215041338: 15 µl & NSI 050515HVOC: 15 µl 
 Pct Recovery = 68%  Analysis Date = 04/28/16 
 SpikeMix = ChemService 3818700: 15 µl & Supelco LC13544: 15 µl 
 Pct Recovery = 91%  Analysis Date = 08/24/15 
 SpikeMix = ERA 0601-15-05: 15 µl & Supelco LC13544: 15 µl 
 Pct Recovery = 100%  Analysis Date = 07/30/15 
 SpikeMix = Supelco LC13544: 15 µl & NSI 050515HVOC: 15 µl 
 Pct Recovery = 87%  Analysis Date = 05/14/15 
 SpikeMix = ChemService 3818700: 15 µl & Supelco LC13544: 15 µl 
 Pct Recovery = 100%  Analysis Date = 12/13/14 
 SpikeMix = Accu 214031128: 10 µl & NSI 031814: 10 µl 
 Pct Recovery = 148%  Analysis Date = 10/21/14 
 SpikeMix = ERA 0321-14-05A: 10 µl & Accu 214031128: 10 µl 
 Pct Recovery = 122%  Analysis Date = 09/11/14 
 SpikeMix = Accu 214031128: 10 µl & Abs 032014: 10 µl 
 Pct Recovery = 139%  Analysis Date = 05/20/14 
 SpikeMix = ChemService 2615700: 10 µl & Accu 214031128: 10 µl 
 Pct Recovery = 132%  Analysis Date = 11/22/14 
 SpikeMix = ChemService 2615700: 10 µl & Supelco LC06437: 10 µl 
 Pct Recovery = 149%  Analysis Date = 09/06/14 
 SpikeMix = ERA 0321-14-05: 10 µl & Supelco LC06437: 10 µl 
 Pct Recovery = 163%  Analysis Date = 06/17/14 
 SpikeMix = Supelco LC06437: 10 µl & Abs 032014: 10 µl 
 Pct Recovery = 132%  Analysis Date = 02/12/16 
 SpikeMix = ERA 0601-15-05: 10 µl & Accu 215041338: 10 µl 
 Pct Recovery = 88%  Analysis Date = 01/05/16 
 SpikeMix = Accu 215041338: 10 µl & Abs 040315: 10 µl 
 Pct Recovery = 118%  Analysis Date = 05/20/15 
 SpikeMix = ChemService 3818700: 10 µl & Accu 215041338: 10 µl 
 Pct Recovery = 92%  Analysis Date = 03/22/16 
 SpikeMix = Supelco LC13544: 10 µl & NSI 050515HVOC: 10 µl 
 Pct Recovery = 106%  Analysis Date = 12/10/15 
 SpikeMix = ChemService 3818700: 10 µl & Supelco LC13544: 10 µl 
 Pct Recovery = 93%  Analysis Date = 05/05/15 
 SpikeMix = Supelco LC13544: 10 µl & Abs 040315: 10 µl 
 Pct Recovery = 95%  Analysis Date = 07/27/16 
 Pct Recovery = 93%  Analysis Date = 07/22/16 
 Pct Recovery = 93%  Analysis Date = 07/22/16 
 Pct Recovery = 93%  Analysis Date = 07/18/16 
 Pct Recovery = 93%  Analysis Date = 07/18/16 
 Pct Recovery = 93%  Analysis Date = 07/14/16 
 Pct Recovery = 93%  Analysis Date = 07/14/16 
 Pct Recovery = 93%  Analysis Date = 07/10/16 
 Pct Recovery = 93%  Analysis Date = 07/10/16 
 Pct Recovery = 93%  Analysis Date = 07/06/16 
 Pct Recovery = 93%  Analysis Date = 07/06/16 
 Pct Recovery = 93%  Analysis Date = 07/02/16 
 Pct Recovery = 93%  Analysis Date = 07/02/16 
 Pct Recovery = 93%  Analysis Date = 06/28/16 
 Pct Recovery = 93%  Analysis Date = 06/28/16 
 Pct Recovery = 93%  Analysis Date = 06/24/16 
 Pct Recovery = 93%  Analysis Date = 06/24/16 
 Pct Recovery = 93%  Analysis Date = 06/20/16 
 Pct Recovery = 94%  Analysis Date = 06/20/16 
 Pct Recovery = 94%  Analysis Date = 06/16/16 
 Pct Recovery = 94%  Analysis Date = 06/16/16 
 Pct Recovery = 94%  Analysis Date = 06/12/16 
 Pct Recovery = 94%  Analysis Date = 06/12/16 
 Pct Recovery = 94%  Analysis Date = 06/08/16 
 Pct Recovery = 94%  Analysis Date = 06/08/16 
 Pct Recovery = 94%  Analysis Date = 06/04/16 
 Pct Recovery = 94%  Analysis Date = 06/04/16 
 Pct Recovery = 94%  Analysis Date = 05/31/16 
 Pct Recovery = 94%  Analysis Date = 05/31/16 
 Pct Recovery = 94%  Analysis Date = 05/27/16 
 Pct Recovery = 94%  Analysis Date = 05/27/16 
 Pct Recovery = 94%  Analysis Date = 05/23/16 
 Pct Recovery = 94%  Analysis Date = 05/23/16 
 Pct Recovery = 94%  Analysis Date = 05/18/16 
 Pct Recovery = 94%  Analysis Date = 05/18/16 
 Pct Recovery = 94%  Analysis Date = 05/14/16 
 Pct Recovery = 94%  Analysis Date = 05/14/16 
 Pct Recovery = 94%  Analysis Date = 05/10/16 
 Pct Recovery = 94%  Analysis Date = 05/10/16 
 Pct Recovery = 94%  Analysis Date = 05/06/16 
 Pct Recovery = 94%  Analysis Date = 05/06/16 
 Pct Recovery = 94%  Analysis Date = 05/02/16 
 Pct Recovery = 94%  Analysis Date = 05/02/16 
 Pct Recovery = 94%  Analysis Date = 04/28/16 
 Pct Recovery = 95%  Analysis Date = 04/28/16 
 Pct Recovery = 95%  Analysis Date = 04/24/16 
 Pct Recovery = 95%  Analysis Date = 04/24/16 
 Pct Recovery = 95%  Analysis Date = 04/20/16 
 Pct Recovery = 95%  Analysis Date = 04/20/16 
 Pct Recovery = 95%  Analysis Date = 04/16/16 
 Pct Recovery = 95%  Analysis Date = 04/16/16 
 Pct Recovery = 95%  Analysis Date = 04/12/16 
 Pct Recovery = 95%  Analysis Date = 04/12/16 
 Pct Recovery = 95%  Analysis Date = 04/08/16 
 Pct Recovery = 95%  Analysis Date = 04/08/16 
 Pct Recovery = 95%  Analysis Date = 04/04/16 
 Pct Recovery = 95%  Analysis Date = 04/04/16 
 Pct Recovery = 95%  Analysis Date = 03/31/16 
 Pct Recovery = 95%  Analysis Date = 03/31/16 
 Pct Recovery = 95%  Analysis Date = 03/27/16 
 Pct Recovery = 95%  Analysis Date = 03/27/16 
 Pct Recovery = 95%  Analysis Date = 03/23/16 
 Pct Recovery = 95%  Analysis Date = 03/23/16 
 Pct Recovery = 95%  Analysis Date = 03/19/16 
 Pct Recovery = 95%  Analysis Date = 03/19/16 
 Pct Recovery = 95%  Analysis Date = 03/15/16 
 Pct Recovery = 95%  Analysis Date = 03/15/16 
 Pct Recovery = 95%  Analysis Date = 03/10/16 
 Pct Recovery = 95%  Analysis Date = 03/10/16 
 Pct Recovery = 95%  Analysis Date = 03/06/16 
 Pct Recovery = 95%  Analysis Date = 03/06/16 
 Pct Recovery = 95%  Analysis Date = 03/02/16 
 Pct Recovery = 96%  Analysis Date = 03/02/16 
 Pct Recovery = 96%  Analysis Date = 02/27/16 
 Pct Recovery = 96%  Analysis Date = 02/27/16 
 Pct Recovery = 96%  Analysis Date = 02/23/16 
 Pct Recovery = 96%  Analysis Date = 02/23/16 
 Pct Recovery = 96%  Analysis Date = 02/19/16 
 Pct Recovery = 96%  Analysis Date = 02/19/16 
 Pct Recovery = 96%  Analysis Date = 02/15/16 
 Pct Recovery = 96%  Analysis Date = 02/15/16 
 Pct Recovery = 96%  Analysis Date = 02/11/16 
 Pct Recovery = 96%  Analysis Date = 02/11/16 
 Pct Recovery = 96%  Analysis Date = 02/07/16 
 Pct Recovery = 96%  Analysis Date = 02/07/16 
 Pct Recovery = 96%  Analysis Date = 02/03/16 
 Pct Recovery = 96%  Analysis Date = 02/03/16 
 Pct Recovery = 96%  Analysis Date = 01/30/16 
 Pct Recovery = 96%  Analysis Date = 01/30/16 
 Pct Recovery = 96%  Analysis Date = 01/26/16 
 Pct Recovery = 96%  Analysis Date = 01/26/16 
 Pct Recovery = 96%  Analysis Date = 01/22/16 
 Pct Recovery = 96%  Analysis Date = 01/22/16 
 Pct Recovery = 96%  Analysis Date = 01/18/16 
 Pct Recovery = 96%  Analysis Date = 01/18/16 
 Pct Recovery = 96%  Analysis Date = 01/14/16 
 Pct Recovery = 96%  Analysis Date = 01/14/16 
 Pct Recovery = 96%  Analysis Date = 01/10/16 
 Pct Recovery = 96%  Analysis Date = 01/10/16 
 Pct Recovery = 96%  Analysis Date = 01/06/16 
 Pct Recovery = 96%  Analysis Date = 01/06/16 
 Pct Recovery = 96%  Analysis Date = 01/01/16 
 Pct Recovery = 96%  Analysis Date = 01/01/16 
 Pct Recovery = 96%  Analysis Date = 12/28/15 
 Pct Recovery = 96%  Analysis Date = 12/28/15 
 Pct Recovery = 96%  Analysis Date = 12/24/15 
 Pct Recovery = 96%  Analysis Date = 12/24/15 
 Pct Recovery = 96%  Analysis Date = 12/20/15 
 Pct Recovery = 96%  Analysis Date = 12/20/15 
 Pct Recovery = 96%  Analysis Date = 12/16/15 
 Pct Recovery = 96%  Analysis Date = 12/16/15 
 Pct Recovery = 96%  Analysis Date = 12/12/15 
 Pct Recovery = 96%  Analysis Date = 12/12/15 
 Pct Recovery = 96%  Analysis Date = 12/08/15 
 Pct Recovery = 96%  Analysis Date = 12/08/15 
 Pct Recovery = 96%  Analysis Date = 12/04/15 
 Pct Recovery = 96%  Analysis Date = 12/04/15 
 Pct Recovery = 96%  Analysis Date = 11/30/15 
 Pct Recovery = 96%  Analysis Date = 11/30/15 
 Pct Recovery = 96%  Analysis Date = 11/26/15 
 Pct Recovery = 96%  Analysis Date = 11/26/15 
 Pct Recovery = 96%  Analysis Date = 11/22/15 
 Pct Recovery = 97%  Analysis Date = 11/22/15 
 Pct Recovery = 97%  Analysis Date = 11/18/15 
 Pct Recovery = 97%  Analysis Date = 11/18/15 
 Pct Recovery = 97%  Analysis Date = 11/14/15 
 Pct Recovery = 97%  Analysis Date = 11/14/15 
 Pct Recovery = 97%  Analysis Date = 11/10/15 
 Pct Recovery = 97%  Analysis Date = 11/10/15 
 Pct Recovery = 97%  Analysis Date = 11/06/15 
 Pct Recovery = 97%  Analysis Date = 11/06/15 
 Pct Recovery = 97%  Analysis Date = 11/02/15 
 Pct Recovery = 97%  Analysis Date = 11/02/15 
 Pct Recovery = 97%  Analysis Date = 10/28/15 
 Pct Recovery = 97%  Analysis Date = 10/28/15 
 Pct Recovery = 97%  Analysis Date = 10/24/15 
 Pct Recovery = 97%  Analysis Date = 10/24/15 
 Pct Recovery = 97%  Analysis Date = 10/20/15 
 Pct Recovery = 97%  Analysis Date = 10/20/15 
 Pct Recovery = 97%  Analysis Date = 10/16/15 
 Pct Recovery = 97%  Analysis Date = 10/16/15 
 Pct Recovery = 97%  Analysis Date = 10/12/15 
 Pct Recovery = 98%  Analysis Date = 10/12/15 
 Pct Recovery = 98%  Analysis Date = 10/08/15 
 Pct Recovery = 98%  Analysis Date = 10/08/15 
 Pct Recovery = 98%  Analysis Date = 10/04/15 
 Pct Recovery = 98%  Analysis Date = 10/04/15 
 Pct Recovery = 98%  Analysis Date = 09/30/15 
 Pct Recovery = 98%  Analysis Date = 09/30/15 
 Pct Recovery = 98%  Analysis Date = 09/26/15 
 Pct Recovery = 98%  Analysis Date = 09/26/15 
 Pct Recovery = 98%  Analysis Date = 09/22/15 
 Pct Recovery = 98%  Analysis Date = 09/22/15 
 Pct Recovery = 98%  Analysis Date = 09/18/15 
 Pct Recovery = 99%  Analysis Date = 09/18/15 
 Pct Recovery = 99%  Analysis Date = 09/14/15 
 Pct Recovery = 99%  Analysis Date = 09/14/15 
 Pct Recovery = 99%  Analysis Date = 09/10/15 
 Pct Recovery = 99%  Analysis Date = 09/10/15 
 Pct Recovery = 99%  Analysis Date = 09/06/15 
 Pct Recovery = 99%  Analysis Date = 09/06/15 
 Pct Recovery = 99%  Analysis Date = 09/02/15 
 Pct Recovery = 99%  Analysis Date = 09/02/15 
 Pct Recovery = 99%  Analysis Date = 08/29/15 
 Pct Recovery = 100%  Analysis Date = 08/29/15 
 Pct Recovery = 100%  Analysis Date = 08/25/15 
 Pct Recovery = 100%  Analysis Date = 08/25/15 
 Pct Recovery = 100%  Analysis Date = 08/20/15 
 Pct Recovery = 100%  Analysis Date = 08/20/15 
 Pct Recovery = 100%  Analysis Date = 08/16/15 
 Pct Recovery = 101%  Analysis Date = 08/16/15 
 Pct Recovery = 101%  Analysis Date = 08/12/15 
 Pct Recovery = 101%  Analysis Date = 08/12/15 
 Pct Recovery = 101%  Analysis Date = 08/08/15 
 Pct Recovery = 102%  Analysis Date = 08/08/15 
 Pct Recovery = 102%  Analysis Date = 08/04/15 
 Pct Recovery = 103%  Analysis Date = 08/04/15 
 Pct Recovery = 103%  Analysis Date = 07/31/15 
 Pct Recovery = 103%  Analysis Date = 07/31/15 
 Pct Recovery = 103%  Analysis Date = 07/27/15 
 Pct Recovery = 104%  Analysis Date = 07/27/15 
 Pct Recovery = 104%  Analysis Date = 07/23/15 
 Pct Recovery = 104%  Analysis Date = 07/23/15 
 Pct Recovery = 104%  Analysis Date = 07/19/15 
 Pct Recovery = 105%  Analysis Date = 07/19/15 
 Pct Recovery = 105%  Analysis Date = 07/15/15 
 Pct Recovery = 106%  Analysis Date = 07/15/15 
 Pct Recovery = 106%  Analysis Date = 07/11/15 
 Pct Recovery = 106%  Analysis Date = 07/11/15 
 Pct Recovery = 106%  Analysis Date = 07/07/15 
 Pct Recovery = 107%  Analysis Date = 07/07/15 
 Pct Recovery = 107%  Analysis Date = 07/03/15 
 Pct Recovery = 107%  Analysis Date = 07/03/15 
 Pct Recovery = 107%  Analysis Date = 06/29/15 
 Pct Recovery = 108%  Analysis Date = 06/29/15 
 Pct Recovery = 108%  Analysis Date = 06/25/15 
 Pct Recovery = 109%  Analysis Date = 06/25/15 
 Pct Recovery = 109%  Analysis Date = 06/21/15 
 Pct Recovery = 109%  Analysis Date = 06/21/15 
 Pct Recovery = 109%  Analysis Date = 06/17/15 
 Pct Recovery = 110%  Analysis Date = 06/17/15 
 Pct Recovery = 110%  Analysis Date = 06/12/15 
 Pct Recovery = 111%  Analysis Date = 06/12/15 
 Pct Recovery = 111%  Analysis Date = 06/08/15 
 Pct Recovery = 111%  Analysis Date = 06/08/15 
 Pct Recovery = 111%  Analysis Date = 06/04/15 
 Pct Recovery = 112%  Analysis Date = 06/04/15 
 Pct Recovery = 112%  Analysis Date = 05/31/15 
 Pct Recovery = 113%  Analysis Date = 05/31/15 
 Pct Recovery = 113%  Analysis Date = 05/27/15 
 Pct Recovery = 114%  Analysis Date = 05/27/15 
 Pct Recovery = 114%  Analysis Date = 05/23/15 
 Pct Recovery = 114%  Analysis Date = 05/23/15 
 Pct Recovery = 114%  Analysis Date = 05/19/15 
 Pct Recovery = 115%  Analysis Date = 05/19/15 
 Pct Recovery = 115%  Analysis Date = 05/15/15 
 Pct Recovery = 116%  Analysis Date = 05/15/15 
 Pct Recovery = 116%  Analysis Date = 05/11/15 
 Pct Recovery = 116%  Analysis Date = 05/11/15 
 Pct Recovery = 116%  Analysis Date = 05/07/15 
 Pct Recovery = 117%  Analysis Date = 05/07/15 
 Pct Recovery = 117%  Analysis Date = 05/03/15 
 Pct Recovery = 118%  Analysis Date = 05/03/15 
 Pct Recovery = 118%  Analysis Date = 04/29/15 
 Pct Recovery = 118%  Analysis Date = 04/29/15 
 Pct Recovery = 118%  Analysis Date = 04/25/15 
 Pct Recovery = 119%  Analysis Date = 04/25/15 
 Pct Recovery = 119%  Analysis Date = 04/21/15 
 Pct Recovery = 120%  Analysis Date = 04/21/15 
 Pct Recovery = 120%  Analysis Date = 04/17/15 
 Pct Recovery = 120%  Analysis Date = 04/17/15 
 Pct Recovery = 120%  Analysis Date = 04/13/15 
 Pct Recovery = 121%  Analysis Date = 04/13/15 
 Pct Recovery = 121%  Analysis Date = 04/08/15 
 Pct Recovery = 122%  Analysis Date = 04/08/15 
 Pct Recovery = 122%  Analysis Date = 04/04/15 
 Pct Recovery = 122%  Analysis Date = 04/04/15 
 Pct Recovery = 122%  Analysis Date = 03/31/15 
 Pct Recovery = 123%  Analysis Date = 03/31/15 
 Pct Recovery = 123%  Analysis Date = 03/27/15 
 Pct Recovery = 124%  Analysis Date = 03/27/15 
 Pct Recovery = 124%  Analysis Date = 03/23/15 
 Pct Recovery = 124%  Analysis Date = 03/23/15 
 Pct Recovery = 124%  Analysis Date = 03/19/15 
 Pct Recovery = 125%  Analysis Date = 03/19/15 
 Pct Recovery = 125%  Analysis Date = 03/15/15 
 Pct Recovery = 126%  Analysis Date = 03/15/15 
 Pct Recovery = 126%  Analysis Date = 03/11/15 
 Pct Recovery = 126%  Analysis Date = 03/11/15 
 Pct Recovery = 126%  Analysis Date = 03/07/15 
 Pct Recovery = 127%  Analysis Date = 03/07/15 
 Pct Recovery = 127%  Analysis Date = 03/03/15 
 Pct Recovery = 128%  Analysis Date = 03/03/15 
 Pct Recovery = 128%  Analysis Date = 02/27/15 
 Pct Recovery = 129%  Analysis Date = 02/27/15 
 Pct Recovery = 129%  Analysis Date = 02/23/15 
 Pct Recovery = 130%  Analysis Date = 02/23/15 
 Pct Recovery = 130%  Analysis Date = 02/19/15 
 Pct Recovery = 131%  Analysis Date = 02/19/15 
 Pct Recovery = 131%  Analysis Date = 02/15/15 
 Pct Recovery = 131%  Analysis Date = 02/15/15 
 Pct Recovery = 131%  Analysis Date = 02/11/15 
 Pct Recovery = 132%  Analysis Date = 02/11/15 
 Pct Recovery = 132%  Analysis Date = 02/07/15 
 Pct Recovery = 133%  Analysis Date = 02/07/15 
 Pct Recovery = 133%  Analysis Date = 02/03/15 
 Pct Recovery = 134%  Analysis Date = 02/03/15 
 Pct Recovery = 134%  Analysis Date = 01/29/15 
 Pct Recovery = 135%  Analysis Date = 01/29/15 
 Pct Recovery = 135%  Analysis Date = 01/25/15 
 Pct Recovery = 136%  Analysis Date = 01/25/15 
 Pct Recovery = 136%  Analysis Date = 01/21/15 
 Pct Recovery = 136%  Analysis Date = 01/21/15 
 Pct Recovery = 136%  Analysis Date = 01/17/15 
 Pct Recovery = 137%  Analysis Date = 01/17/15 
 Pct Recovery = 137%  Analysis Date = 01/13/15 
 Pct Recovery = 138%  Analysis Date = 01/13/15 
 Pct Recovery = 138%  Analysis Date = 01/09/15 
 Pct Recovery = 139%  Analysis Date = 01/09/15 
 Pct Recovery = 139%  Analysis Date = 01/05/15 
 Pct Recovery = 140%  Analysis Date = 01/05/15 
 Pct Recovery = 140%  Analysis Date = 01/01/15 
 Pct Recovery = 141%  Analysis Date = 01/01/15 
 Pct Recovery = 141%  Analysis Date = 12/28/14 
 Pct Recovery = 141%  Analysis Date = 12/28/14 
 Pct Recovery = 141%  Analysis Date = 12/24/14 
 Pct Recovery = 142%  Analysis Date = 12/24/14 
 Pct Recovery = 142%  Analysis Date = 12/20/14 
 Pct Recovery = 143%  Analysis Date = 12/20/14 
 Pct Recovery = 143%  Analysis Date = 12/16/14 
 Pct Recovery = 144%  Analysis Date = 12/16/14 
 Pct Recovery = 144%  Analysis Date = 12/12/14 
 Pct Recovery = 145%  Analysis Date = 12/12/14 
 Pct Recovery = 145%  Analysis Date = 12/08/14 
 Pct Recovery = 146%  Analysis Date = 12/08/14 
 Pct Recovery = 146%  Analysis Date = 12/04/14 
 Pct Recovery = 146%  Analysis Date = 12/04/14 
 Pct Recovery = 146%  Analysis Date = 11/30/14 
 Pct Recovery = 147%  Analysis Date = 11/30/14 
 Pct Recovery = 147%  Analysis Date = 11/26/14 
 Pct Recovery = 148%  Analysis Date = 11/26/14 
 Pct Recovery = 148%  Analysis Date = 11/21/14 
 Pct Recovery = 149%  Analysis Date = 11/21/14 
 Pct Recovery = 149%  Analysis Date = 11/17/14 
 Pct Recovery = 149%  Analysis Date = 11/17/14 
 Pct Recovery = 149%  Analysis Date = 11/13/14 
 Pct Recovery = 148%  Analysis Date = 11/13/14 
 Pct Recovery = 148%  Analysis Date = 11/09/14 
 Pct Recovery = 148%  Analysis Date = 11/09/14 
 Pct Recovery = 148%  Analysis Date = 11/05/14 
 Pct Recovery = 148%  Analysis Date = 11/05/14 
 Pct Recovery = 148%  Analysis Date = 11/01/14 
 Pct Recovery = 148%  Analysis Date = 11/01/14 
 Pct Recovery = 148%  Analysis Date = 10/28/14 
 Pct Recovery = 147%  Analysis Date = 10/28/14 
 Pct Recovery = 147%  Analysis Date = 10/24/14 
 Pct Recovery = 147%  Analysis Date = 10/24/14 
 Pct Recovery = 147%  Analysis Date = 10/20/14 
 Pct Recovery = 147%  Analysis Date = 10/20/14 
 Pct Recovery = 147%  Analysis Date = 10/16/14 
 Pct Recovery = 147%  Analysis Date = 10/16/14 
 Pct Recovery = 147%  Analysis Date = 10/12/14 
 Pct Recovery = 146%  Analysis Date = 10/12/14 
 Pct Recovery = 146%  Analysis Date = 10/08/14 
 Pct Recovery = 146%  Analysis Date = 10/08/14 
 Pct Recovery = 146%  Analysis Date = 10/04/14 
 Pct Recovery = 146%  Analysis Date = 10/04/14 
 Pct Recovery = 146%  Analysis Date = 09/30/14 
 Pct Recovery = 145%  Analysis Date = 09/30/14 
 Pct Recovery = 145%  Analysis Date = 09/26/14 
 Pct Recovery = 145%  Analysis Date = 09/26/14 
 Pct Recovery = 145%  Analysis Date = 09/22/14 
 Pct Recovery = 145%  Analysis Date = 09/22/14 
 Pct Recovery = 145%  Analysis Date = 09/17/14 
 Pct Recovery = 145%  Analysis Date = 09/17/14 
 Pct Recovery = 145%  Analysis Date = 09/13/14 
 Pct Recovery = 144%  Analysis Date = 09/13/14 
 Pct Recovery = 144%  Analysis Date = 09/09/14 
 Pct Recovery = 144%  Analysis Date = 09/09/14 
 Pct Recovery = 144%  Analysis Date = 09/05/14 
 Pct Recovery = 144%  Analysis Date = 09/05/14 
 Pct Recovery = 144%  Analysis Date = 09/01/14 
 Pct Recovery = 143%  Analysis Date = 09/01/14 
 Pct Recovery = 143%  Analysis Date = 08/28/14 
 Pct Recovery = 143%  Analysis Date = 08/28/14 
 Pct Recovery = 143%  Analysis Date = 08/24/14 
 Pct Recovery = 142%  Analysis Date = 08/24/14 
 Pct Recovery = 142%  Analysis Date = 08/20/14 
 Pct Recovery = 142%  Analysis Date = 08/20/14 
 Pct Recovery = 142%  Analysis Date = 08/16/14 
 Pct Recovery = 142%  Analysis Date = 08/16/14 
 Pct Recovery = 142%  Analysis Date = 08/12/14 
 Pct Recovery = 141%  Analysis Date = 08/12/14 
 Pct Recovery = 141%  Analysis Date = 08/08/14 
 Pct Recovery = 141%  Analysis Date = 08/08/14 
 Pct Recovery = 141%  Analysis Date = 08/04/14 
 Pct Recovery = 140%  Analysis Date = 08/04/14 
 Pct Recovery = 140%  Analysis Date = 07/31/14 
 Pct Recovery = 140%  Analysis Date = 07/31/14 
 Pct Recovery = 140%  Analysis Date = 07/27/14 
 Pct Recovery = 140%  Analysis Date = 07/27/14 
 Pct Recovery = 140%  Analysis Date = 07/23/14 
 Pct Recovery = 139%  Analysis Date = 07/23/14 
 Pct Recovery = 139%  Analysis Date = 07/19/14 
 Pct Recovery = 139%  Analysis Date = 07/19/14 
 Pct Recovery = 139%  Analysis Date = 07/15/14 
 Pct Recovery = 138%  Analysis Date = 07/15/14 
 Pct Recovery = 138%  Analysis Date = 07/10/14 
 Pct Recovery = 138%  Analysis Date = 07/10/14 
 Pct Recovery = 138%  Analysis Date = 07/06/14 
 Pct Recovery = 137%  Analysis Date = 07/06/14 
 Pct Recovery = 137%  Analysis Date = 07/02/14 
 Pct Recovery = 137%  Analysis Date = 07/02/14 
 Pct Recovery = 137%  Analysis Date = 06/28/14 
 Pct Recovery = 136%  Analysis Date = 06/28/14 
 Pct Recovery = 136%  Analysis Date = 06/24/14 
 Pct Recovery = 136%  Analysis Date = 06/24/14 
 Pct Recovery = 136%  Analysis Date = 06/20/14 
 Pct Recovery = 136%  Analysis Date = 06/20/14 
 Pct Recovery = 136%  Analysis Date = 06/16/14 
 Pct Recovery = 135%  Analysis Date = 06/16/14 
 Pct Recovery = 135%  Analysis Date = 06/12/14 
 Pct Recovery = 135%  Analysis Date = 06/12/14 
 Pct Recovery = 135%  Analysis Date = 06/08/14 
 Pct Recovery = 134%  Analysis Date = 06/08/14 
 Pct Recovery = 134%  Analysis Date = 06/04/14 
 Pct Recovery = 134%  Analysis Date = 06/04/14 
 Pct Recovery = 134%  Analysis Date = 05/31/14 
 Pct Recovery = 133%  Analysis Date = 05/31/14 
 Pct Recovery = 133%  Analysis Date = 05/27/14 
 Pct Recovery = 133%  Analysis Date = 05/27/14 
 Pct Recovery = 133%  Analysis Date = 05/23/14 
 Pct Recovery = 132%  Analysis Date = 05/23/14 
 Pct Recovery = 132%  Analysis Date = 05/19/14 
 Pct Recovery = 132%  Analysis Date = 05/19/14 
 Pct Recovery = 132%  Analysis Date = 05/15/14 
 Pct Recovery = 131%  Analysis Date = 05/15/14 
 Pct Recovery = 131%  Analysis Date = 05/11/14 
 Pct Recovery = 131%  Analysis Date = 05/11/14 
 Pct Recovery = 131%  Analysis Date = 05/07/14 
 Pct Recovery = 130%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
2-ETHOXYETHYL ACETATE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 31 118% 31% 111% 34%
Total 31 118% 31% 111% 34%

Sample Statistics
2-ETHOXYETHYL ACETATE

Characteristic N % % Basis
Plotted 31 82% Spiked
Estimated Values 3 8% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 38 .  
False Negatives 7 18% 7 out of 38
Not Spiked 17 .  
False Positives 1 6% 1 out of 17

BQS OBSP Determination:
2-HEXANONE, 5-METHYL-
METHOD: 4437 , TESTIDCODE: 77179GM016
Open Data Set

 Analysis Date = 07/11/14 
 SpikeMix = ChemService 2615700: 20 µl & Accu 214031128: 20 µl 
 Pct Recovery = 115%  Analysis Date = 07/03/14 
 SpikeMix = Abs 032014: 20 µl & ChemService 2615700: 20 µl 
 Pct Recovery = 95%  Analysis Date = 06/07/14 
 SpikeMix = ChemService 2615700: 20 µl & Supelco LC06437: 20 µl 
 Pct Recovery = 105%  Analysis Date = 06/06/14 
 SpikeMix = NSI 031814: 20 µl & ChemService 2615700: 20 µl 
 Pct Recovery = 92%  Analysis Date = 01/10/15 
 SpikeMix = Abs 032014: 20 µl & ERA 0321-14-05A: 20 µl 
 Pct Recovery = 97%  Analysis Date = 08/13/14 
 SpikeMix = ERA 0321-14-05: 20 µl & Accu 214031128: 20 µl 
 Pct Recovery = 119%  Analysis Date = 10/09/15 
 SpikeMix = ERA 0601-15-05: 25 µl & Accu 215041338: 25 µl 
 Pct Recovery = 98%  Analysis Date = 10/09/15 
 SpikeMix = Supelco LC13544: 25 µl & NSI 050515HVOC: 25 µl 
 Pct Recovery = 116%  Analysis Date = 06/26/15 
 SpikeMix = ChemService 3818700: 25 µl & Accu 215041338: 25 µl 
 Pct Recovery = 98%  Analysis Date = 08/12/16 
 SpikeMix = Accu 216041354: 15 µl & Abs 060916HVOC: 15 µl 
 Pct Recovery = 80%  Analysis Date = 04/28/16 
 SpikeMix = ChemService 3818700: 15 µl & Supelco LC13544: 15 µl 
 Pct Recovery = 90%  Analysis Date = 11/25/15 
 SpikeMix = Accu 215041338: 15 µl & Abs 040315: 15 µl 
 Pct Recovery = 101%  Analysis Date = 09/05/15 
 SpikeMix = Accu 215041338: 15 µl & NSI 050515HVOC: 15 µl 
 Pct Recovery = 91%  Analysis Date = 08/24/15 
 SpikeMix = ERA 0601-15-05: 15 µl & Supelco LC13544: 15 µl 
 Pct Recovery = 111%  Analysis Date = 07/30/15 
 SpikeMix = Supelco LC13544: 15 µl & NSI 050515HVOC: 15 µl 
 Pct Recovery = 100%  Analysis Date = 05/14/15 
 SpikeMix = ChemService 3818700: 15 µl & Supelco LC13544: 15 µl 
 Pct Recovery = 99%  Analysis Date = 11/22/14 
 SpikeMix = ChemService 2615700: 10 µl & Supelco LC06437: 10 µl 
 Pct Recovery = 94%  Analysis Date = 07/30/14 
 SpikeMix = NSI 031814: 10 µl & ChemService 2615700: 10 µl 
 Pct Recovery = 113%  Analysis Date = 05/20/14 
 SpikeMix = ChemService 2615700: 10 µl & Accu 214031128: 10 µl 
 Pct Recovery = 104%  Analysis Date = 04/25/15 
 SpikeMix = Abs 032014: 10 µl & ERA 0321-14-05A: 10 µl 
 Pct Recovery = 112%  Analysis Date = 10/21/14 
 SpikeMix = ERA 0321-14-05A: 10 µl & Accu 214031128: 10 µl 
 Pct Recovery = 102%  Analysis Date = 09/06/14 
 SpikeMix = ERA 0321-14-05: 10 µl & Supelco LC06437: 10 µl 
 Pct Recovery = 129%  Analysis Date = 03/22/16 
 SpikeMix = Supelco LC13544: 10 µl & NSI 050515HVOC: 10 µl 
 Pct Recovery = 115%  Analysis Date = 02/12/16 
 SpikeMix = ERA 0601-15-05: 10 µl & Accu 215041338: 10 µl 
 Pct Recovery = 102%  Analysis Date = 01/05/16 
 SpikeMix = Accu 215041338: 10 µl & Abs 040315: 10 µl 
 Pct Recovery = 98%  Analysis Date = 12/10/15 
 SpikeMix = ChemService 3818700: 10 µl & Supelco LC13544: 10 µl 
 Pct Recovery = 110%  Analysis Date = 05/20/15 
 SpikeMix = ChemService 3818700: 10 µl & Accu 215041338: 10 µl 
 Pct Recovery = 86%  Analysis Date = 05/05/15 
 SpikeMix = Supelco LC13544: 10 µl & Abs 040315: 10 µl 
 Pct Recovery = 96%  Analysis Date = 08/12/16 
 Pct Recovery = 87%  Analysis Date = 08/07/16 
 Pct Recovery = 88%  Analysis Date = 08/07/16 
 Pct Recovery = 88%  Analysis Date = 08/03/16 
 Pct Recovery = 88%  Analysis Date = 08/03/16 
 Pct Recovery = 88%  Analysis Date = 07/30/16 
 Pct Recovery = 88%  Analysis Date = 07/30/16 
 Pct Recovery = 88%  Analysis Date = 07/26/16 
 Pct Recovery = 89%  Analysis Date = 07/26/16 
 Pct Recovery = 89%  Analysis Date = 07/22/16 
 Pct Recovery = 89%  Analysis Date = 07/22/16 
 Pct Recovery = 89%  Analysis Date = 07/18/16 
 Pct Recovery = 89%  Analysis Date = 07/18/16 
 Pct Recovery = 89%  Analysis Date = 07/14/16 
 Pct Recovery = 90%  Analysis Date = 07/14/16 
 Pct Recovery = 90%  Analysis Date = 07/10/16 
 Pct Recovery = 90%  Analysis Date = 07/10/16 
 Pct Recovery = 90%  Analysis Date = 07/06/16 
 Pct Recovery = 90%  Analysis Date = 07/06/16 
 Pct Recovery = 90%  Analysis Date = 07/02/16 
 Pct Recovery = 90%  Analysis Date = 07/02/16 
 Pct Recovery = 90%  Analysis Date = 06/28/16 
 Pct Recovery = 91%  Analysis Date = 06/28/16 
 Pct Recovery = 91%  Analysis Date = 06/24/16 
 Pct Recovery = 91%  Analysis Date = 06/24/16 
 Pct Recovery = 91%  Analysis Date = 06/20/16 
 Pct Recovery = 91%  Analysis Date = 06/20/16 
 Pct Recovery = 91%  Analysis Date = 06/15/16 
 Pct Recovery = 92%  Analysis Date = 06/15/16 
 Pct Recovery = 92%  Analysis Date = 06/11/16 
 Pct Recovery = 92%  Analysis Date = 06/11/16 
 Pct Recovery = 92%  Analysis Date = 06/07/16 
 Pct Recovery = 92%  Analysis Date = 06/07/16 
 Pct Recovery = 92%  Analysis Date = 06/03/16 
 Pct Recovery = 92%  Analysis Date = 06/03/16 
 Pct Recovery = 92%  Analysis Date = 05/30/16 
 Pct Recovery = 93%  Analysis Date = 05/30/16 
 Pct Recovery = 93%  Analysis Date = 05/26/16 
 Pct Recovery = 93%  Analysis Date = 05/26/16 
 Pct Recovery = 93%  Analysis Date = 05/22/16 
 Pct Recovery = 93%  Analysis Date = 05/22/16 
 Pct Recovery = 93%  Analysis Date = 05/18/16 
 Pct Recovery = 94%  Analysis Date = 05/18/16 
 Pct Recovery = 94%  Analysis Date = 05/14/16 
 Pct Recovery = 94%  Analysis Date = 05/14/16 
 Pct Recovery = 94%  Analysis Date = 05/10/16 
 Pct Recovery = 94%  Analysis Date = 05/10/16 
 Pct Recovery = 94%  Analysis Date = 05/06/16 
 Pct Recovery = 94%  Analysis Date = 05/06/16 
 Pct Recovery = 94%  Analysis Date = 05/02/16 
 Pct Recovery = 95%  Analysis Date = 05/02/16 
 Pct Recovery = 95%  Analysis Date = 04/28/16 
 Pct Recovery = 95%  Analysis Date = 04/28/16 
 Pct Recovery = 95%  Analysis Date = 04/23/16 
 Pct Recovery = 95%  Analysis Date = 04/23/16 
 Pct Recovery = 95%  Analysis Date = 04/19/16 
 Pct Recovery = 96%  Analysis Date = 04/19/16 
 Pct Recovery = 96%  Analysis Date = 04/15/16 
 Pct Recovery = 96%  Analysis Date = 04/15/16 
 Pct Recovery = 96%  Analysis Date = 04/11/16 
 Pct Recovery = 96%  Analysis Date = 04/11/16 
 Pct Recovery = 96%  Analysis Date = 04/07/16 
 Pct Recovery = 96%  Analysis Date = 04/07/16 
 Pct Recovery = 96%  Analysis Date = 04/03/16 
 Pct Recovery = 97%  Analysis Date = 04/03/16 
 Pct Recovery = 97%  Analysis Date = 03/30/16 
 Pct Recovery = 97%  Analysis Date = 03/30/16 
 Pct Recovery = 97%  Analysis Date = 03/26/16 
 Pct Recovery = 97%  Analysis Date = 03/26/16 
 Pct Recovery = 97%  Analysis Date = 03/22/16 
 Pct Recovery = 98%  Analysis Date = 03/22/16 
 Pct Recovery = 98%  Analysis Date = 03/18/16 
 Pct Recovery = 98%  Analysis Date = 03/18/16 
 Pct Recovery = 98%  Analysis Date = 03/14/16 
 Pct Recovery = 98%  Analysis Date = 03/14/16 
 Pct Recovery = 98%  Analysis Date = 03/10/16 
 Pct Recovery = 98%  Analysis Date = 03/10/16 
 Pct Recovery = 98%  Analysis Date = 03/06/16 
 Pct Recovery = 99%  Analysis Date = 03/06/16 
 Pct Recovery = 99%  Analysis Date = 03/02/16 
 Pct Recovery = 99%  Analysis Date = 03/02/16 
 Pct Recovery = 99%  Analysis Date = 02/26/16 
 Pct Recovery = 99%  Analysis Date = 02/26/16 
 Pct Recovery = 99%  Analysis Date = 02/22/16 
 Pct Recovery = 100%  Analysis Date = 02/22/16 
 Pct Recovery = 100%  Analysis Date = 02/18/16 
 Pct Recovery = 100%  Analysis Date = 02/18/16 
 Pct Recovery = 100%  Analysis Date = 02/14/16 
 Pct Recovery = 100%  Analysis Date = 02/14/16 
 Pct Recovery = 100%  Analysis Date = 02/10/16 
 Pct Recovery = 100%  Analysis Date = 02/10/16 
 Pct Recovery = 100%  Analysis Date = 02/06/16 
 Pct Recovery = 101%  Analysis Date = 02/06/16 
 Pct Recovery = 101%  Analysis Date = 02/02/16 
 Pct Recovery = 101%  Analysis Date = 02/02/16 
 Pct Recovery = 101%  Analysis Date = 01/29/16 
 Pct Recovery = 101%  Analysis Date = 01/29/16 
 Pct Recovery = 101%  Analysis Date = 01/25/16 
 Pct Recovery = 101%  Analysis Date = 01/25/16 
 Pct Recovery = 101%  Analysis Date = 01/21/16 
 Pct Recovery = 101%  Analysis Date = 01/21/16 
 Pct Recovery = 101%  Analysis Date = 01/17/16 
 Pct Recovery = 102%  Analysis Date = 01/17/16 
 Pct Recovery = 102%  Analysis Date = 01/13/16 
 Pct Recovery = 102%  Analysis Date = 01/13/16 
 Pct Recovery = 102%  Analysis Date = 01/09/16 
 Pct Recovery = 102%  Analysis Date = 01/09/16 
 Pct Recovery = 102%  Analysis Date = 01/04/16 
 Pct Recovery = 102%  Analysis Date = 01/04/16 
 Pct Recovery = 102%  Analysis Date = 12/31/15 
 Pct Recovery = 102%  Analysis Date = 12/31/15 
 Pct Recovery = 102%  Analysis Date = 12/27/15 
 Pct Recovery = 102%  Analysis Date = 12/27/15 
 Pct Recovery = 102%  Analysis Date = 12/23/15 
 Pct Recovery = 103%  Analysis Date = 12/23/15 
 Pct Recovery = 103%  Analysis Date = 12/19/15 
 Pct Recovery = 103%  Analysis Date = 12/19/15 
 Pct Recovery = 103%  Analysis Date = 12/15/15 
 Pct Recovery = 103%  Analysis Date = 12/15/15 
 Pct Recovery = 103%  Analysis Date = 12/11/15 
 Pct Recovery = 103%  Analysis Date = 12/11/15 
 Pct Recovery = 103%  Analysis Date = 12/07/15 
 Pct Recovery = 103%  Analysis Date = 12/07/15 
 Pct Recovery = 103%  Analysis Date = 12/03/15 
 Pct Recovery = 103%  Analysis Date = 12/03/15 
 Pct Recovery = 103%  Analysis Date = 11/29/15 
 Pct Recovery = 103%  Analysis Date = 11/29/15 
 Pct Recovery = 103%  Analysis Date = 11/25/15 
 Pct Recovery = 103%  Analysis Date = 11/25/15 
 Pct Recovery = 103%  Analysis Date = 11/21/15 
 Pct Recovery = 103%  Analysis Date = 11/21/15 
 Pct Recovery = 103%  Analysis Date = 11/17/15 
 Pct Recovery = 103%  Analysis Date = 11/17/15 
 Pct Recovery = 103%  Analysis Date = 11/12/15 
 Pct Recovery = 103%  Analysis Date = 11/12/15 
 Pct Recovery = 103%  Analysis Date = 11/08/15 
 Pct Recovery = 103%  Analysis Date = 11/08/15 
 Pct Recovery = 103%  Analysis Date = 11/04/15 
 Pct Recovery = 103%  Analysis Date = 11/04/15 
 Pct Recovery = 103%  Analysis Date = 10/31/15 
 Pct Recovery = 103%  Analysis Date = 10/31/15 
 Pct Recovery = 103%  Analysis Date = 10/27/15 
 Pct Recovery = 103%  Analysis Date = 10/27/15 
 Pct Recovery = 103%  Analysis Date = 10/23/15 
 Pct Recovery = 103%  Analysis Date = 10/23/15 
 Pct Recovery = 103%  Analysis Date = 10/19/15 
 Pct Recovery = 103%  Analysis Date = 10/19/15 
 Pct Recovery = 103%  Analysis Date = 10/15/15 
 Pct Recovery = 102%  Analysis Date = 10/15/15 
 Pct Recovery = 102%  Analysis Date = 10/11/15 
 Pct Recovery = 102%  Analysis Date = 10/11/15 
 Pct Recovery = 102%  Analysis Date = 10/07/15 
 Pct Recovery = 102%  Analysis Date = 10/07/15 
 Pct Recovery = 102%  Analysis Date = 10/03/15 
 Pct Recovery = 102%  Analysis Date = 10/03/15 
 Pct Recovery = 102%  Analysis Date = 09/29/15 
 Pct Recovery = 102%  Analysis Date = 09/29/15 
 Pct Recovery = 102%  Analysis Date = 09/25/15 
 Pct Recovery = 102%  Analysis Date = 09/25/15 
 Pct Recovery = 102%  Analysis Date = 09/21/15 
 Pct Recovery = 102%  Analysis Date = 09/21/15 
 Pct Recovery = 102%  Analysis Date = 09/16/15 
 Pct Recovery = 102%  Analysis Date = 09/16/15 
 Pct Recovery = 102%  Analysis Date = 09/12/15 
 Pct Recovery = 102%  Analysis Date = 09/12/15 
 Pct Recovery = 102%  Analysis Date = 09/08/15 
 Pct Recovery = 102%  Analysis Date = 09/08/15 
 Pct Recovery = 102%  Analysis Date = 09/04/15 
 Pct Recovery = 101%  Analysis Date = 09/04/15 
 Pct Recovery = 101%  Analysis Date = 08/31/15 
 Pct Recovery = 101%  Analysis Date = 08/31/15 
 Pct Recovery = 101%  Analysis Date = 08/27/15 
 Pct Recovery = 101%  Analysis Date = 08/27/15 
 Pct Recovery = 101%  Analysis Date = 08/23/15 
 Pct Recovery = 101%  Analysis Date = 08/23/15 
 Pct Recovery = 101%  Analysis Date = 08/19/15 
 Pct Recovery = 101%  Analysis Date = 08/19/15 
 Pct Recovery = 101%  Analysis Date = 08/15/15 
 Pct Recovery = 101%  Analysis Date = 08/15/15 
 Pct Recovery = 101%  Analysis Date = 08/11/15 
 Pct Recovery = 101%  Analysis Date = 08/11/15 
 Pct Recovery = 101%  Analysis Date = 08/07/15 
 Pct Recovery = 101%  Analysis Date = 08/07/15 
 Pct Recovery = 101%  Analysis Date = 08/03/15 
 Pct Recovery = 101%  Analysis Date = 08/03/15 
 Pct Recovery = 101%  Analysis Date = 07/30/15 
 Pct Recovery = 101%  Analysis Date = 07/30/15 
 Pct Recovery = 101%  Analysis Date = 07/25/15 
 Pct Recovery = 100%  Analysis Date = 07/25/15 
 Pct Recovery = 100%  Analysis Date = 07/21/15 
 Pct Recovery = 100%  Analysis Date = 07/21/15 
 Pct Recovery = 100%  Analysis Date = 07/17/15 
 Pct Recovery = 100%  Analysis Date = 07/17/15 
 Pct Recovery = 100%  Analysis Date = 07/13/15 
 Pct Recovery = 100%  Analysis Date = 07/13/15 
 Pct Recovery = 100%  Analysis Date = 07/09/15 
 Pct Recovery = 100%  Analysis Date = 07/09/15 
 Pct Recovery = 100%  Analysis Date = 07/05/15 
 Pct Recovery = 100%  Analysis Date = 07/05/15 
 Pct Recovery = 100%  Analysis Date = 07/01/15 
 Pct Recovery = 100%  Analysis Date = 07/01/15 
 Pct Recovery = 100%  Analysis Date = 06/27/15 
 Pct Recovery = 100%  Analysis Date = 06/27/15 
 Pct Recovery = 100%  Analysis Date = 06/23/15 
 Pct Recovery = 100%  Analysis Date = 06/23/15 
 Pct Recovery = 100%  Analysis Date = 06/19/15 
 Pct Recovery = 100%  Analysis Date = 06/19/15 
 Pct Recovery = 100%  Analysis Date = 06/15/15 
 Pct Recovery = 100%  Analysis Date = 06/15/15 
 Pct Recovery = 100%  Analysis Date = 06/11/15 
 Pct Recovery = 99%  Analysis Date = 06/11/15 
 Pct Recovery = 99%  Analysis Date = 06/07/15 
 Pct Recovery = 99%  Analysis Date = 06/07/15 
 Pct Recovery = 99%  Analysis Date = 06/02/15 
 Pct Recovery = 99%  Analysis Date = 06/02/15 
 Pct Recovery = 99%  Analysis Date = 05/29/15 
 Pct Recovery = 99%  Analysis Date = 05/29/15 
 Pct Recovery = 99%  Analysis Date = 05/25/15 
 Pct Recovery = 99%  Analysis Date = 05/25/15 
 Pct Recovery = 99%  Analysis Date = 05/21/15 
 Pct Recovery = 99%  Analysis Date = 05/21/15 
 Pct Recovery = 99%  Analysis Date = 05/17/15 
 Pct Recovery = 99%  Analysis Date = 05/17/15 
 Pct Recovery = 99%  Analysis Date = 05/13/15 
 Pct Recovery = 99%  Analysis Date = 05/13/15 
 Pct Recovery = 99%  Analysis Date = 05/09/15 
 Pct Recovery = 99%  Analysis Date = 05/09/15 
 Pct Recovery = 99%  Analysis Date = 05/05/15 
 Pct Recovery = 99%  Analysis Date = 05/05/15 
 Pct Recovery = 99%  Analysis Date = 05/01/15 
 Pct Recovery = 99%  Analysis Date = 05/01/15 
 Pct Recovery = 99%  Analysis Date = 04/27/15 
 Pct Recovery = 99%  Analysis Date = 04/27/15 
 Pct Recovery = 99%  Analysis Date = 04/23/15 
 Pct Recovery = 99%  Analysis Date = 04/23/15 
 Pct Recovery = 99%  Analysis Date = 04/19/15 
 Pct Recovery = 99%  Analysis Date = 04/19/15 
 Pct Recovery = 99%  Analysis Date = 04/15/15 
 Pct Recovery = 100%  Analysis Date = 04/15/15 
 Pct Recovery = 100%  Analysis Date = 04/11/15 
 Pct Recovery = 100%  Analysis Date = 04/11/15 
 Pct Recovery = 100%  Analysis Date = 04/06/15 
 Pct Recovery = 100%  Analysis Date = 04/06/15 
 Pct Recovery = 100%  Analysis Date = 04/02/15 
 Pct Recovery = 100%  Analysis Date = 04/02/15 
 Pct Recovery = 100%  Analysis Date = 03/29/15 
 Pct Recovery = 100%  Analysis Date = 03/29/15 
 Pct Recovery = 100%  Analysis Date = 03/25/15 
 Pct Recovery = 100%  Analysis Date = 03/25/15 
 Pct Recovery = 100%  Analysis Date = 03/21/15 
 Pct Recovery = 100%  Analysis Date = 03/21/15 
 Pct Recovery = 100%  Analysis Date = 03/17/15 
 Pct Recovery = 100%  Analysis Date = 03/17/15 
 Pct Recovery = 100%  Analysis Date = 03/13/15 
 Pct Recovery = 101%  Analysis Date = 03/13/15 
 Pct Recovery = 101%  Analysis Date = 03/09/15 
 Pct Recovery = 101%  Analysis Date = 03/09/15 
 Pct Recovery = 101%  Analysis Date = 03/05/15 
 Pct Recovery = 101%  Analysis Date = 03/05/15 
 Pct Recovery = 101%  Analysis Date = 03/01/15 
 Pct Recovery = 101%  Analysis Date = 03/01/15 
 Pct Recovery = 101%  Analysis Date = 02/25/15 
 Pct Recovery = 101%  Analysis Date = 02/25/15 
 Pct Recovery = 101%  Analysis Date = 02/21/15 
 Pct Recovery = 101%  Analysis Date = 02/21/15 
 Pct Recovery = 101%  Analysis Date = 02/17/15 
 Pct Recovery = 101%  Analysis Date = 02/17/15 
 Pct Recovery = 101%  Analysis Date = 02/12/15 
 Pct Recovery = 101%  Analysis Date = 02/12/15 
 Pct Recovery = 101%  Analysis Date = 02/08/15 
 Pct Recovery = 102%  Analysis Date = 02/08/15 
 Pct Recovery = 102%  Analysis Date = 02/04/15 
 Pct Recovery = 102%  Analysis Date = 02/04/15 
 Pct Recovery = 102%  Analysis Date = 01/31/15 
 Pct Recovery = 102%  Analysis Date = 01/31/15 
 Pct Recovery = 102%  Analysis Date = 01/27/15 
 Pct Recovery = 102%  Analysis Date = 01/27/15 
 Pct Recovery = 102%  Analysis Date = 01/23/15 
 Pct Recovery = 102%  Analysis Date = 01/23/15 
 Pct Recovery = 102%  Analysis Date = 01/19/15 
 Pct Recovery = 102%  Analysis Date = 01/19/15 
 Pct Recovery = 102%  Analysis Date = 01/15/15 
 Pct Recovery = 102%  Analysis Date = 01/15/15 
 Pct Recovery = 102%  Analysis Date = 01/11/15 
 Pct Recovery = 102%  Analysis Date = 01/11/15 
 Pct Recovery = 102%  Analysis Date = 01/07/15 
 Pct Recovery = 102%  Analysis Date = 01/07/15 
 Pct Recovery = 102%  Analysis Date = 01/03/15 
 Pct Recovery = 103%  Analysis Date = 01/03/15 
 Pct Recovery = 103%  Analysis Date = 12/30/14 
 Pct Recovery = 103%  Analysis Date = 12/30/14 
 Pct Recovery = 103%  Analysis Date = 12/26/14 
 Pct Recovery = 103%  Analysis Date = 12/26/14 
 Pct Recovery = 103%  Analysis Date = 12/21/14 
 Pct Recovery = 103%  Analysis Date = 12/21/14 
 Pct Recovery = 103%  Analysis Date = 12/17/14 
 Pct Recovery = 103%  Analysis Date = 12/17/14 
 Pct Recovery = 103%  Analysis Date = 12/13/14 
 Pct Recovery = 103%  Analysis Date = 12/13/14 
 Pct Recovery = 103%  Analysis Date = 12/09/14 
 Pct Recovery = 103%  Analysis Date = 12/09/14 
 Pct Recovery = 103%  Analysis Date = 12/05/14 
 Pct Recovery = 104%  Analysis Date = 12/05/14 
 Pct Recovery = 104%  Analysis Date = 12/01/14 
 Pct Recovery = 104%  Analysis Date = 12/01/14 
 Pct Recovery = 104%  Analysis Date = 11/27/14 
 Pct Recovery = 104%  Analysis Date = 11/27/14 
 Pct Recovery = 104%  Analysis Date = 11/23/14 
 Pct Recovery = 104%  Analysis Date = 11/23/14 
 Pct Recovery = 104%  Analysis Date = 11/19/14 
 Pct Recovery = 104%  Analysis Date = 11/19/14 
 Pct Recovery = 104%  Analysis Date = 11/15/14 
 Pct Recovery = 104%  Analysis Date = 11/15/14 
 Pct Recovery = 104%  Analysis Date = 11/11/14 
 Pct Recovery = 104%  Analysis Date = 11/11/14 
 Pct Recovery = 104%  Analysis Date = 11/07/14 
 Pct Recovery = 105%  Analysis Date = 11/07/14 
 Pct Recovery = 105%  Analysis Date = 11/03/14 
 Pct Recovery = 105%  Analysis Date = 11/03/14 
 Pct Recovery = 105%  Analysis Date = 10/30/14 
 Pct Recovery = 105%  Analysis Date = 10/30/14 
 Pct Recovery = 105%  Analysis Date = 10/25/14 
 Pct Recovery = 105%  Analysis Date = 10/25/14 
 Pct Recovery = 105%  Analysis Date = 10/21/14 
 Pct Recovery = 105%  Analysis Date = 10/21/14 
 Pct Recovery = 105%  Analysis Date = 10/17/14 
 Pct Recovery = 105%  Analysis Date = 10/17/14 
 Pct Recovery = 105%  Analysis Date = 10/13/14 
 Pct Recovery = 105%  Analysis Date = 10/13/14 
 Pct Recovery = 105%  Analysis Date = 10/09/14 
 Pct Recovery = 105%  Analysis Date = 10/09/14 
 Pct Recovery = 105%  Analysis Date = 10/05/14 
 Pct Recovery = 105%  Analysis Date = 10/05/14 
 Pct Recovery = 105%  Analysis Date = 10/01/14 
 Pct Recovery = 105%  Analysis Date = 10/01/14 
 Pct Recovery = 105%  Analysis Date = 09/27/14 
 Pct Recovery = 105%  Analysis Date = 09/27/14 
 Pct Recovery = 105%  Analysis Date = 09/23/14 
 Pct Recovery = 106%  Analysis Date = 09/23/14 
 Pct Recovery = 106%  Analysis Date = 09/19/14 
 Pct Recovery = 106%  Analysis Date = 09/19/14 
 Pct Recovery = 106%  Analysis Date = 09/15/14 
 Pct Recovery = 106%  Analysis Date = 09/15/14 
 Pct Recovery = 106%  Analysis Date = 09/11/14 
 Pct Recovery = 106%  Analysis Date = 09/11/14 
 Pct Recovery = 106%  Analysis Date = 09/07/14 
 Pct Recovery = 106%  Analysis Date = 09/07/14 
 Pct Recovery = 106%  Analysis Date = 09/02/14 
 Pct Recovery = 106%  Analysis Date = 09/02/14 
 Pct Recovery = 106%  Analysis Date = 08/29/14 
 Pct Recovery = 106%  Analysis Date = 08/29/14 
 Pct Recovery = 106%  Analysis Date = 08/25/14 
 Pct Recovery = 106%  Analysis Date = 08/25/14 
 Pct Recovery = 106%  Analysis Date = 08/21/14 
 Pct Recovery = 106%  Analysis Date = 08/21/14 
 Pct Recovery = 106%  Analysis Date = 08/17/14 
 Pct Recovery = 106%  Analysis Date = 08/17/14 
 Pct Recovery = 106%  Analysis Date = 08/13/14 
 Pct Recovery = 106%  Analysis Date = 08/13/14 
 Pct Recovery = 106%  Analysis Date = 08/09/14 
 Pct Recovery = 106%  Analysis Date = 08/09/14 
 Pct Recovery = 106%  Analysis Date = 08/05/14 
 Pct Recovery = 106%  Analysis Date = 08/05/14 
 Pct Recovery = 106%  Analysis Date = 08/01/14 
 Pct Recovery = 106%  Analysis Date = 08/01/14 
 Pct Recovery = 106%  Analysis Date = 07/28/14 
 Pct Recovery = 106%  Analysis Date = 07/28/14 
 Pct Recovery = 106%  Analysis Date = 07/24/14 
 Pct Recovery = 106%  Analysis Date = 07/24/14 
 Pct Recovery = 106%  Analysis Date = 07/20/14 
 Pct Recovery = 106%  Analysis Date = 07/20/14 
 Pct Recovery = 106%  Analysis Date = 07/16/14 
 Pct Recovery = 106%  Analysis Date = 07/16/14 
 Pct Recovery = 106%  Analysis Date = 07/11/14 
 Pct Recovery = 107%  Analysis Date = 07/11/14 
 Pct Recovery = 107%  Analysis Date = 07/07/14 
 Pct Recovery = 107%  Analysis Date = 07/07/14 
 Pct Recovery = 107%  Analysis Date = 07/03/14 
 Pct Recovery = 107%  Analysis Date = 07/03/14 
 Pct Recovery = 107%  Analysis Date = 06/29/14 
 Pct Recovery = 107%  Analysis Date = 06/29/14 
 Pct Recovery = 107%  Analysis Date = 06/25/14 
 Pct Recovery = 107%  Analysis Date = 06/25/14 
 Pct Recovery = 107%  Analysis Date = 06/21/14 
 Pct Recovery = 107%  Analysis Date = 06/21/14 
 Pct Recovery = 107%  Analysis Date = 06/17/14 
 Pct Recovery = 107%  Analysis Date = 06/17/14 
 Pct Recovery = 107%  Analysis Date = 06/13/14 
 Pct Recovery = 107%  Analysis Date = 06/13/14 
 Pct Recovery = 107%  Analysis Date = 06/09/14 
 Pct Recovery = 107%  Analysis Date = 06/09/14 
 Pct Recovery = 107%  Analysis Date = 06/05/14 
 Pct Recovery = 107%  Analysis Date = 06/05/14 
 Pct Recovery = 107%  Analysis Date = 06/01/14 
 Pct Recovery = 107%  Analysis Date = 06/01/14 
 Pct Recovery = 107%  Analysis Date = 05/28/14 
 Pct Recovery = 107%  Analysis Date = 05/28/14 
 Pct Recovery = 107%  Analysis Date = 05/24/14 
 Pct Recovery = 107%  Analysis Date = 05/24/14 
 Pct Recovery = 107%  Analysis Date = 05/20/14 
 Pct Recovery = 107%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
2-HEXANONE, 5-METHYL-

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 28 102% 11% 100% 12%
Total 28 102% 11% 100% 12%

Sample Statistics
2-HEXANONE, 5-METHYL-

Characteristic N % % Basis
Plotted 28 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 28 .  
False Negatives 0 0% 0 out of 28
Not Spiked 20 .  
False Positives 0 0% 0 out of 20

BQS OBSP Determination:
2-NITROPROPANE
METHOD: 4437 , TESTIDCODE: 77076GM016
Open Data Set

 Analysis Date = 07/29/16 
 SpikeMix = Supelco LC20145V: 40 µl & NSI 041516: 40 µl & NSI 041416HVOC: 40 µl 
 Pct Recovery = 90%  Analysis Date = 07/06/16 
 SpikeMix = Accu 216041354: 40 µl & NSI 041516: 40 µl & NSI 041416HVOC: 40 µl 
 Pct Recovery = 81%  Analysis Date = 08/11/16 
 SpikeMix = Phenova B20160303: 25 µl & Supelco LC20145V: 25 µl & NSI 041416HVOC: 25 µl 
 Pct Recovery = 91%  Analysis Date = 05/21/16 
 SpikeMix = Supelco LC20145V: 25 µl & NSI 041516: 25 µl & NSI 041416HVOC: 25 µl 
 Pct Recovery = 90%  Analysis Date = 03/19/15 
 SpikeMix = Supelco LC06437: 20 µl & NSI 031814: 20 µl 
 Pct Recovery = 83%  Analysis Date = 08/20/14 
 SpikeMix = Supelco LC06437: 20 µl & Abs 032014: 20 µl 
 Pct Recovery = 83%  Analysis Date = 06/07/14 
 SpikeMix = ChemService 2615700: 20 µl & Supelco LC06437: 20 µl 
 Pct Recovery = 93%  Analysis Date = 08/13/14 
 SpikeMix = ERA 0321-14-05: 20 µl & Accu 214031128: 20 µl 
 Pct Recovery = 88%  Analysis Date = 07/23/14 
 SpikeMix = Accu 214031128: 20 µl & Abs 032014: 20 µl 
 Pct Recovery = 80%  Analysis Date = 07/11/14 
 SpikeMix = ChemService 2615700: 20 µl & Accu 214031128: 20 µl 
 Pct Recovery = 93%  Analysis Date = 05/07/14 
 SpikeMix = NSI 031814: 20 µl & Accu 214031128: 20 µl 
 Pct Recovery = 81%  Analysis Date = 01/22/16 
 SpikeMix = NSI 050515HVOC: 25 µl & ERA 0601-15-05: 25 µl 
 Pct Recovery = 86%  Analysis Date = 10/09/15 
 SpikeMix = Supelco LC13544: 25 µl & NSI 050515HVOC: 25 µl 
 Pct Recovery = 81%  Analysis Date = 06/25/15 
 SpikeMix = ChemService 3818700: 25 µl & NSI 050515HVOC: 25 µl 
 Pct Recovery = 89%  Analysis Date = 07/27/16 
 SpikeMix = ChemService 5082800: 15 µl & Supelco LC20145V: 15 µl & Accu 216041225: 15 µl 
 Pct Recovery = 82%  Analysis Date = 08/12/16 
 SpikeMix = Accu 216041354: 15 µl & Abs 060916HVOC: 15 µl 
 Pct Recovery = 78%  Analysis Date = 07/06/16 
 SpikeMix = Phenova B20160303: 15 µl & Accu 216041354: 15 µl & NSI 041416HVOC: 15 µl 
 Pct Recovery = 77%  Analysis Date = 06/23/16 
 SpikeMix = . 
 Pct Recovery = 80%  Analysis Date = 05/20/16 
 SpikeMix = Accu 216041354: 15 µl & NSI 041516: 15 µl & Accu 216041225: 15 µl 
 Pct Recovery = 88%  Analysis Date = 11/25/15 
 SpikeMix = Accu 215041338: 15 µl & Abs 040315: 15 µl 
 Pct Recovery = 90%  Analysis Date = 09/24/15 
 SpikeMix = Abs 040315: 15 µl & ERA 0601-15-05: 15 µl 
 Pct Recovery = 96%  Analysis Date = 09/05/15 
 SpikeMix = Accu 215041338: 15 µl & NSI 050515HVOC: 15 µl 
 Pct Recovery = 78%  Analysis Date = 07/30/15 
 SpikeMix = Supelco LC13544: 15 µl & NSI 050515HVOC: 15 µl 
 Pct Recovery = 81%  Analysis Date = 06/16/15 
 SpikeMix = ChemService 3818700: 15 µl & NSI 050515HVOC: 15 µl 
 Pct Recovery = 91%  Analysis Date = 11/22/14 
 SpikeMix = ChemService 2615700: 10 µl & Supelco LC06437: 10 µl 
 Pct Recovery = 91%  Analysis Date = 09/06/14 
 SpikeMix = ERA 0321-14-05: 10 µl & Supelco LC06437: 10 µl 
 Pct Recovery = 100%  Analysis Date = 06/17/14 
 SpikeMix = Supelco LC06437: 10 µl & Abs 032014: 10 µl 
 Pct Recovery = 93%  Analysis Date = 12/13/14 
 SpikeMix = Accu 214031128: 10 µl & NSI 031814: 10 µl 
 Pct Recovery = 83%  Analysis Date = 10/21/14 
 SpikeMix = ERA 0321-14-05A: 10 µl & Accu 214031128: 10 µl 
 Pct Recovery = 98%  Analysis Date = 09/11/14 
 SpikeMix = Accu 214031128: 10 µl & Abs 032014: 10 µl 
 Pct Recovery = 83%  Analysis Date = 05/20/14 
 SpikeMix = ChemService 2615700: 10 µl & Accu 214031128: 10 µl 
 Pct Recovery = 107%  Analysis Date = 04/09/16 
 SpikeMix = Abs 040315: 10 µl & ChemService 3818700: 10 µl 
 Pct Recovery = 104%  Analysis Date = 03/22/16 
 SpikeMix = Supelco LC13544: 10 µl & NSI 050515HVOC: 10 µl 
 Pct Recovery = 89%  Analysis Date = 01/05/16 
 SpikeMix = Accu 215041338: 10 µl & Abs 040315: 10 µl 
 Pct Recovery = 99%  Analysis Date = 12/05/15 
 SpikeMix = NSI 050515HVOC: 10 µl & ERA 0601-15-05: 10 µl 
 Pct Recovery = 91%  Analysis Date = 10/23/15 
 SpikeMix = Abs 040315: 10 µl & ChemService 3818700: 10 µl 
 Pct Recovery = 101%  Analysis Date = 08/14/15 
 SpikeMix = Abs 040315: 10 µl & ERA 0601-15-05: 10 µl 
 Pct Recovery = 91%  Analysis Date = 05/05/15 
 SpikeMix = Supelco LC13544: 10 µl & Abs 040315: 10 µl 
 Pct Recovery = 99%  Analysis Date = 08/11/16 
 Pct Recovery = 84%  Analysis Date = 08/07/16 
 Pct Recovery = 84%  Analysis Date = 08/07/16 
 Pct Recovery = 84%  Analysis Date = 08/03/16 
 Pct Recovery = 84%  Analysis Date = 08/03/16 
 Pct Recovery = 84%  Analysis Date = 07/30/16 
 Pct Recovery = 84%  Analysis Date = 07/30/16 
 Pct Recovery = 84%  Analysis Date = 07/26/16 
 Pct Recovery = 85%  Analysis Date = 07/26/16 
 Pct Recovery = 85%  Analysis Date = 07/22/16 
 Pct Recovery = 85%  Analysis Date = 07/22/16 
 Pct Recovery = 85%  Analysis Date = 07/18/16 
 Pct Recovery = 85%  Analysis Date = 07/18/16 
 Pct Recovery = 85%  Analysis Date = 07/14/16 
 Pct Recovery = 85%  Analysis Date = 07/14/16 
 Pct Recovery = 85%  Analysis Date = 07/09/16 
 Pct Recovery = 85%  Analysis Date = 07/09/16 
 Pct Recovery = 85%  Analysis Date = 07/05/16 
 Pct Recovery = 85%  Analysis Date = 07/05/16 
 Pct Recovery = 85%  Analysis Date = 07/01/16 
 Pct Recovery = 85%  Analysis Date = 07/01/16 
 Pct Recovery = 85%  Analysis Date = 06/27/16 
 Pct Recovery = 86%  Analysis Date = 06/27/16 
 Pct Recovery = 86%  Analysis Date = 06/23/16 
 Pct Recovery = 86%  Analysis Date = 06/23/16 
 Pct Recovery = 86%  Analysis Date = 06/19/16 
 Pct Recovery = 86%  Analysis Date = 06/19/16 
 Pct Recovery = 86%  Analysis Date = 06/15/16 
 Pct Recovery = 86%  Analysis Date = 06/15/16 
 Pct Recovery = 86%  Analysis Date = 06/10/16 
 Pct Recovery = 86%  Analysis Date = 06/10/16 
 Pct Recovery = 86%  Analysis Date = 06/06/16 
 Pct Recovery = 86%  Analysis Date = 06/06/16 
 Pct Recovery = 86%  Analysis Date = 06/02/16 
 Pct Recovery = 86%  Analysis Date = 06/02/16 
 Pct Recovery = 86%  Analysis Date = 05/29/16 
 Pct Recovery = 87%  Analysis Date = 05/29/16 
 Pct Recovery = 87%  Analysis Date = 05/25/16 
 Pct Recovery = 87%  Analysis Date = 05/25/16 
 Pct Recovery = 87%  Analysis Date = 05/21/16 
 Pct Recovery = 87%  Analysis Date = 05/21/16 
 Pct Recovery = 87%  Analysis Date = 05/17/16 
 Pct Recovery = 87%  Analysis Date = 05/17/16 
 Pct Recovery = 87%  Analysis Date = 05/12/16 
 Pct Recovery = 87%  Analysis Date = 05/12/16 
 Pct Recovery = 87%  Analysis Date = 05/08/16 
 Pct Recovery = 87%  Analysis Date = 05/08/16 
 Pct Recovery = 87%  Analysis Date = 05/04/16 
 Pct Recovery = 87%  Analysis Date = 05/04/16 
 Pct Recovery = 87%  Analysis Date = 04/30/16 
 Pct Recovery = 88%  Analysis Date = 04/30/16 
 Pct Recovery = 88%  Analysis Date = 04/26/16 
 Pct Recovery = 88%  Analysis Date = 04/26/16 
 Pct Recovery = 88%  Analysis Date = 04/22/16 
 Pct Recovery = 88%  Analysis Date = 04/22/16 
 Pct Recovery = 88%  Analysis Date = 04/18/16 
 Pct Recovery = 88%  Analysis Date = 04/18/16 
 Pct Recovery = 88%  Analysis Date = 04/13/16 
 Pct Recovery = 88%  Analysis Date = 04/13/16 
 Pct Recovery = 88%  Analysis Date = 04/09/16 
 Pct Recovery = 88%  Analysis Date = 04/09/16 
 Pct Recovery = 88%  Analysis Date = 04/05/16 
 Pct Recovery = 88%  Analysis Date = 04/05/16 
 Pct Recovery = 88%  Analysis Date = 04/01/16 
 Pct Recovery = 89%  Analysis Date = 04/01/16 
 Pct Recovery = 89%  Analysis Date = 03/28/16 
 Pct Recovery = 89%  Analysis Date = 03/28/16 
 Pct Recovery = 89%  Analysis Date = 03/24/16 
 Pct Recovery = 89%  Analysis Date = 03/24/16 
 Pct Recovery = 89%  Analysis Date = 03/20/16 
 Pct Recovery = 89%  Analysis Date = 03/20/16 
 Pct Recovery = 89%  Analysis Date = 03/15/16 
 Pct Recovery = 89%  Analysis Date = 03/15/16 
 Pct Recovery = 89%  Analysis Date = 03/11/16 
 Pct Recovery = 89%  Analysis Date = 03/11/16 
 Pct Recovery = 89%  Analysis Date = 03/07/16 
 Pct Recovery = 89%  Analysis Date = 03/07/16 
 Pct Recovery = 89%  Analysis Date = 03/03/16 
 Pct Recovery = 90%  Analysis Date = 03/03/16 
 Pct Recovery = 90%  Analysis Date = 02/28/16 
 Pct Recovery = 90%  Analysis Date = 02/28/16 
 Pct Recovery = 90%  Analysis Date = 02/24/16 
 Pct Recovery = 90%  Analysis Date = 02/24/16 
 Pct Recovery = 90%  Analysis Date = 02/20/16 
 Pct Recovery = 90%  Analysis Date = 02/20/16 
 Pct Recovery = 90%  Analysis Date = 02/15/16 
 Pct Recovery = 90%  Analysis Date = 02/15/16 
 Pct Recovery = 90%  Analysis Date = 02/11/16 
 Pct Recovery = 90%  Analysis Date = 02/11/16 
 Pct Recovery = 90%  Analysis Date = 02/07/16 
 Pct Recovery = 91%  Analysis Date = 02/07/16 
 Pct Recovery = 91%  Analysis Date = 02/03/16 
 Pct Recovery = 91%  Analysis Date = 02/03/16 
 Pct Recovery = 91%  Analysis Date = 01/30/16 
 Pct Recovery = 91%  Analysis Date = 01/30/16 
 Pct Recovery = 91%  Analysis Date = 01/26/16 
 Pct Recovery = 91%  Analysis Date = 01/26/16 
 Pct Recovery = 91%  Analysis Date = 01/22/16 
 Pct Recovery = 91%  Analysis Date = 01/22/16 
 Pct Recovery = 91%  Analysis Date = 01/17/16 
 Pct Recovery = 91%  Analysis Date = 01/17/16 
 Pct Recovery = 91%  Analysis Date = 01/13/16 
 Pct Recovery = 91%  Analysis Date = 01/13/16 
 Pct Recovery = 91%  Analysis Date = 01/09/16 
 Pct Recovery = 91%  Analysis Date = 01/09/16 
 Pct Recovery = 91%  Analysis Date = 01/05/16 
 Pct Recovery = 91%  Analysis Date = 01/05/16 
 Pct Recovery = 91%  Analysis Date = 01/01/16 
 Pct Recovery = 91%  Analysis Date = 01/01/16 
 Pct Recovery = 91%  Analysis Date = 12/28/15 
 Pct Recovery = 91%  Analysis Date = 12/28/15 
 Pct Recovery = 91%  Analysis Date = 12/24/15 
 Pct Recovery = 91%  Analysis Date = 12/24/15 
 Pct Recovery = 91%  Analysis Date = 12/20/15 
 Pct Recovery = 91%  Analysis Date = 12/20/15 
 Pct Recovery = 91%  Analysis Date = 12/15/15 
 Pct Recovery = 91%  Analysis Date = 12/15/15 
 Pct Recovery = 91%  Analysis Date = 12/11/15 
 Pct Recovery = 91%  Analysis Date = 12/11/15 
 Pct Recovery = 91%  Analysis Date = 12/07/15 
 Pct Recovery = 91%  Analysis Date = 12/07/15 
 Pct Recovery = 91%  Analysis Date = 12/03/15 
 Pct Recovery = 91%  Analysis Date = 12/03/15 
 Pct Recovery = 91%  Analysis Date = 11/29/15 
 Pct Recovery = 91%  Analysis Date = 11/29/15 
 Pct Recovery = 91%  Analysis Date = 11/25/15 
 Pct Recovery = 91%  Analysis Date = 11/25/15 
 Pct Recovery = 91%  Analysis Date = 11/21/15 
 Pct Recovery = 91%  Analysis Date = 11/21/15 
 Pct Recovery = 91%  Analysis Date = 11/16/15 
 Pct Recovery = 91%  Analysis Date = 11/16/15 
 Pct Recovery = 91%  Analysis Date = 11/12/15 
 Pct Recovery = 91%  Analysis Date = 11/12/15 
 Pct Recovery = 91%  Analysis Date = 11/08/15 
 Pct Recovery = 90%  Analysis Date = 11/08/15 
 Pct Recovery = 90%  Analysis Date = 11/04/15 
 Pct Recovery = 90%  Analysis Date = 11/04/15 
 Pct Recovery = 90%  Analysis Date = 10/31/15 
 Pct Recovery = 90%  Analysis Date = 10/31/15 
 Pct Recovery = 90%  Analysis Date = 10/27/15 
 Pct Recovery = 90%  Analysis Date = 10/27/15 
 Pct Recovery = 90%  Analysis Date = 10/23/15 
 Pct Recovery = 90%  Analysis Date = 10/23/15 
 Pct Recovery = 90%  Analysis Date = 10/18/15 
 Pct Recovery = 90%  Analysis Date = 10/18/15 
 Pct Recovery = 90%  Analysis Date = 10/14/15 
 Pct Recovery = 90%  Analysis Date = 10/14/15 
 Pct Recovery = 90%  Analysis Date = 10/10/15 
 Pct Recovery = 90%  Analysis Date = 10/10/15 
 Pct Recovery = 90%  Analysis Date = 10/06/15 
 Pct Recovery = 90%  Analysis Date = 10/06/15 
 Pct Recovery = 90%  Analysis Date = 10/02/15 
 Pct Recovery = 90%  Analysis Date = 10/02/15 
 Pct Recovery = 90%  Analysis Date = 09/28/15 
 Pct Recovery = 90%  Analysis Date = 09/28/15 
 Pct Recovery = 90%  Analysis Date = 09/24/15 
 Pct Recovery = 90%  Analysis Date = 09/24/15 
 Pct Recovery = 90%  Analysis Date = 09/19/15 
 Pct Recovery = 90%  Analysis Date = 09/19/15 
 Pct Recovery = 90%  Analysis Date = 09/15/15 
 Pct Recovery = 90%  Analysis Date = 09/15/15 
 Pct Recovery = 90%  Analysis Date = 09/11/15 
 Pct Recovery = 90%  Analysis Date = 09/11/15 
 Pct Recovery = 90%  Analysis Date = 09/07/15 
 Pct Recovery = 90%  Analysis Date = 09/07/15 
 Pct Recovery = 90%  Analysis Date = 09/03/15 
 Pct Recovery = 90%  Analysis Date = 09/03/15 
 Pct Recovery = 90%  Analysis Date = 08/30/15 
 Pct Recovery = 90%  Analysis Date = 08/30/15 
 Pct Recovery = 90%  Analysis Date = 08/26/15 
 Pct Recovery = 90%  Analysis Date = 08/26/15 
 Pct Recovery = 90%  Analysis Date = 08/21/15 
 Pct Recovery = 90%  Analysis Date = 08/21/15 
 Pct Recovery = 90%  Analysis Date = 08/17/15 
 Pct Recovery = 90%  Analysis Date = 08/17/15 
 Pct Recovery = 90%  Analysis Date = 08/13/15 
 Pct Recovery = 89%  Analysis Date = 08/13/15 
 Pct Recovery = 89%  Analysis Date = 08/09/15 
 Pct Recovery = 89%  Analysis Date = 08/09/15 
 Pct Recovery = 89%  Analysis Date = 08/05/15 
 Pct Recovery = 89%  Analysis Date = 08/05/15 
 Pct Recovery = 89%  Analysis Date = 08/01/15 
 Pct Recovery = 89%  Analysis Date = 08/01/15 
 Pct Recovery = 89%  Analysis Date = 07/28/15 
 Pct Recovery = 89%  Analysis Date = 07/28/15 
 Pct Recovery = 89%  Analysis Date = 07/23/15 
 Pct Recovery = 89%  Analysis Date = 07/23/15 
 Pct Recovery = 89%  Analysis Date = 07/19/15 
 Pct Recovery = 89%  Analysis Date = 07/19/15 
 Pct Recovery = 89%  Analysis Date = 07/15/15 
 Pct Recovery = 89%  Analysis Date = 07/15/15 
 Pct Recovery = 89%  Analysis Date = 07/11/15 
 Pct Recovery = 89%  Analysis Date = 07/11/15 
 Pct Recovery = 89%  Analysis Date = 07/07/15 
 Pct Recovery = 89%  Analysis Date = 07/07/15 
 Pct Recovery = 89%  Analysis Date = 07/03/15 
 Pct Recovery = 89%  Analysis Date = 07/03/15 
 Pct Recovery = 89%  Analysis Date = 06/29/15 
 Pct Recovery = 89%  Analysis Date = 06/29/15 
 Pct Recovery = 89%  Analysis Date = 06/24/15 
 Pct Recovery = 89%  Analysis Date = 06/24/15 
 Pct Recovery = 89%  Analysis Date = 06/20/15 
 Pct Recovery = 89%  Analysis Date = 06/20/15 
 Pct Recovery = 89%  Analysis Date = 06/16/15 
 Pct Recovery = 89%  Analysis Date = 06/16/15 
 Pct Recovery = 89%  Analysis Date = 06/12/15 
 Pct Recovery = 89%  Analysis Date = 06/12/15 
 Pct Recovery = 89%  Analysis Date = 06/08/15 
 Pct Recovery = 89%  Analysis Date = 06/08/15 
 Pct Recovery = 89%  Analysis Date = 06/04/15 
 Pct Recovery = 89%  Analysis Date = 06/04/15 
 Pct Recovery = 89%  Analysis Date = 05/31/15 
 Pct Recovery = 89%  Analysis Date = 05/31/15 
 Pct Recovery = 89%  Analysis Date = 05/27/15 
 Pct Recovery = 89%  Analysis Date = 05/27/15 
 Pct Recovery = 89%  Analysis Date = 05/22/15 
 Pct Recovery = 89%  Analysis Date = 05/22/15 
 Pct Recovery = 89%  Analysis Date = 05/18/15 
 Pct Recovery = 89%  Analysis Date = 05/18/15 
 Pct Recovery = 89%  Analysis Date = 05/14/15 
 Pct Recovery = 89%  Analysis Date = 05/14/15 
 Pct Recovery = 89%  Analysis Date = 05/10/15 
 Pct Recovery = 89%  Analysis Date = 05/10/15 
 Pct Recovery = 89%  Analysis Date = 05/06/15 
 Pct Recovery = 89%  Analysis Date = 05/06/15 
 Pct Recovery = 89%  Analysis Date = 05/02/15 
 Pct Recovery = 89%  Analysis Date = 05/02/15 
 Pct Recovery = 89%  Analysis Date = 04/28/15 
 Pct Recovery = 89%  Analysis Date = 04/28/15 
 Pct Recovery = 89%  Analysis Date = 04/23/15 
 Pct Recovery = 89%  Analysis Date = 04/23/15 
 Pct Recovery = 89%  Analysis Date = 04/19/15 
 Pct Recovery = 89%  Analysis Date = 04/19/15 
 Pct Recovery = 89%  Analysis Date = 04/15/15 
 Pct Recovery = 89%  Analysis Date = 04/15/15 
 Pct Recovery = 89%  Analysis Date = 04/11/15 
 Pct Recovery = 89%  Analysis Date = 04/11/15 
 Pct Recovery = 89%  Analysis Date = 04/07/15 
 Pct Recovery = 89%  Analysis Date = 04/07/15 
 Pct Recovery = 89%  Analysis Date = 04/03/15 
 Pct Recovery = 89%  Analysis Date = 04/03/15 
 Pct Recovery = 89%  Analysis Date = 03/30/15 
 Pct Recovery = 89%  Analysis Date = 03/30/15 
 Pct Recovery = 89%  Analysis Date = 03/25/15 
 Pct Recovery = 89%  Analysis Date = 03/25/15 
 Pct Recovery = 89%  Analysis Date = 03/21/15 
 Pct Recovery = 89%  Analysis Date = 03/21/15 
 Pct Recovery = 89%  Analysis Date = 03/17/15 
 Pct Recovery = 89%  Analysis Date = 03/17/15 
 Pct Recovery = 89%  Analysis Date = 03/13/15 
 Pct Recovery = 89%  Analysis Date = 03/13/15 
 Pct Recovery = 89%  Analysis Date = 03/09/15 
 Pct Recovery = 89%  Analysis Date = 03/09/15 
 Pct Recovery = 89%  Analysis Date = 03/05/15 
 Pct Recovery = 89%  Analysis Date = 03/05/15 
 Pct Recovery = 89%  Analysis Date = 03/01/15 
 Pct Recovery = 89%  Analysis Date = 03/01/15 
 Pct Recovery = 89%  Analysis Date = 02/24/15 
 Pct Recovery = 89%  Analysis Date = 02/24/15 
 Pct Recovery = 89%  Analysis Date = 02/20/15 
 Pct Recovery = 89%  Analysis Date = 02/20/15 
 Pct Recovery = 89%  Analysis Date = 02/16/15 
 Pct Recovery = 89%  Analysis Date = 02/16/15 
 Pct Recovery = 89%  Analysis Date = 02/12/15 
 Pct Recovery = 89%  Analysis Date = 02/12/15 
 Pct Recovery = 89%  Analysis Date = 02/08/15 
 Pct Recovery = 89%  Analysis Date = 02/08/15 
 Pct Recovery = 89%  Analysis Date = 02/04/15 
 Pct Recovery = 89%  Analysis Date = 02/04/15 
 Pct Recovery = 89%  Analysis Date = 01/31/15 
 Pct Recovery = 89%  Analysis Date = 01/31/15 
 Pct Recovery = 89%  Analysis Date = 01/26/15 
 Pct Recovery = 89%  Analysis Date = 01/26/15 
 Pct Recovery = 89%  Analysis Date = 01/22/15 
 Pct Recovery = 89%  Analysis Date = 01/22/15 
 Pct Recovery = 89%  Analysis Date = 01/18/15 
 Pct Recovery = 89%  Analysis Date = 01/18/15 
 Pct Recovery = 89%  Analysis Date = 01/14/15 
 Pct Recovery = 89%  Analysis Date = 01/14/15 
 Pct Recovery = 89%  Analysis Date = 01/10/15 
 Pct Recovery = 89%  Analysis Date = 01/10/15 
 Pct Recovery = 89%  Analysis Date = 01/06/15 
 Pct Recovery = 89%  Analysis Date = 01/06/15 
 Pct Recovery = 89%  Analysis Date = 01/02/15 
 Pct Recovery = 89%  Analysis Date = 01/02/15 
 Pct Recovery = 89%  Analysis Date = 12/28/14 
 Pct Recovery = 89%  Analysis Date = 12/28/14 
 Pct Recovery = 89%  Analysis Date = 12/24/14 
 Pct Recovery = 89%  Analysis Date = 12/24/14 
 Pct Recovery = 89%  Analysis Date = 12/20/14 
 Pct Recovery = 89%  Analysis Date = 12/20/14 
 Pct Recovery = 89%  Analysis Date = 12/16/14 
 Pct Recovery = 89%  Analysis Date = 12/16/14 
 Pct Recovery = 89%  Analysis Date = 12/12/14 
 Pct Recovery = 89%  Analysis Date = 12/12/14 
 Pct Recovery = 89%  Analysis Date = 12/08/14 
 Pct Recovery = 90%  Analysis Date = 12/08/14 
 Pct Recovery = 90%  Analysis Date = 12/04/14 
 Pct Recovery = 90%  Analysis Date = 12/04/14 
 Pct Recovery = 90%  Analysis Date = 11/29/14 
 Pct Recovery = 90%  Analysis Date = 11/29/14 
 Pct Recovery = 90%  Analysis Date = 11/25/14 
 Pct Recovery = 90%  Analysis Date = 11/25/14 
 Pct Recovery = 90%  Analysis Date = 11/21/14 
 Pct Recovery = 90%  Analysis Date = 11/21/14 
 Pct Recovery = 90%  Analysis Date = 11/17/14 
 Pct Recovery = 90%  Analysis Date = 11/17/14 
 Pct Recovery = 90%  Analysis Date = 11/13/14 
 Pct Recovery = 90%  Analysis Date = 11/13/14 
 Pct Recovery = 90%  Analysis Date = 11/09/14 
 Pct Recovery = 90%  Analysis Date = 11/09/14 
 Pct Recovery = 90%  Analysis Date = 11/05/14 
 Pct Recovery = 90%  Analysis Date = 11/05/14 
 Pct Recovery = 90%  Analysis Date = 11/01/14 
 Pct Recovery = 90%  Analysis Date = 11/01/14 
 Pct Recovery = 90%  Analysis Date = 10/27/14 
 Pct Recovery = 90%  Analysis Date = 10/27/14 
 Pct Recovery = 90%  Analysis Date = 10/23/14 
 Pct Recovery = 90%  Analysis Date = 10/23/14 
 Pct Recovery = 90%  Analysis Date = 10/19/14 
 Pct Recovery = 90%  Analysis Date = 10/19/14 
 Pct Recovery = 90%  Analysis Date = 10/15/14 
 Pct Recovery = 90%  Analysis Date = 10/15/14 
 Pct Recovery = 90%  Analysis Date = 10/11/14 
 Pct Recovery = 90%  Analysis Date = 10/11/14 
 Pct Recovery = 90%  Analysis Date = 10/07/14 
 Pct Recovery = 90%  Analysis Date = 10/07/14 
 Pct Recovery = 90%  Analysis Date = 10/03/14 
 Pct Recovery = 90%  Analysis Date = 10/03/14 
 Pct Recovery = 90%  Analysis Date = 09/28/14 
 Pct Recovery = 90%  Analysis Date = 09/28/14 
 Pct Recovery = 90%  Analysis Date = 09/24/14 
 Pct Recovery = 90%  Analysis Date = 09/24/14 
 Pct Recovery = 90%  Analysis Date = 09/20/14 
 Pct Recovery = 90%  Analysis Date = 09/20/14 
 Pct Recovery = 90%  Analysis Date = 09/16/14 
 Pct Recovery = 90%  Analysis Date = 09/16/14 
 Pct Recovery = 90%  Analysis Date = 09/12/14 
 Pct Recovery = 90%  Analysis Date = 09/12/14 
 Pct Recovery = 90%  Analysis Date = 09/08/14 
 Pct Recovery = 90%  Analysis Date = 09/08/14 
 Pct Recovery = 90%  Analysis Date = 09/04/14 
 Pct Recovery = 90%  Analysis Date = 09/04/14 
 Pct Recovery = 90%  Analysis Date = 08/30/14 
 Pct Recovery = 90%  Analysis Date = 08/30/14 
 Pct Recovery = 90%  Analysis Date = 08/26/14 
 Pct Recovery = 90%  Analysis Date = 08/26/14 
 Pct Recovery = 90%  Analysis Date = 08/22/14 
 Pct Recovery = 90%  Analysis Date = 08/22/14 
 Pct Recovery = 90%  Analysis Date = 08/18/14 
 Pct Recovery = 90%  Analysis Date = 08/18/14 
 Pct Recovery = 90%  Analysis Date = 08/14/14 
 Pct Recovery = 90%  Analysis Date = 08/14/14 
 Pct Recovery = 90%  Analysis Date = 08/10/14 
 Pct Recovery = 90%  Analysis Date = 08/10/14 
 Pct Recovery = 90%  Analysis Date = 08/06/14 
 Pct Recovery = 90%  Analysis Date = 08/06/14 
 Pct Recovery = 90%  Analysis Date = 08/01/14 
 Pct Recovery = 90%  Analysis Date = 08/01/14 
 Pct Recovery = 90%  Analysis Date = 07/28/14 
 Pct Recovery = 90%  Analysis Date = 07/28/14 
 Pct Recovery = 90%  Analysis Date = 07/24/14 
 Pct Recovery = 90%  Analysis Date = 07/24/14 
 Pct Recovery = 90%  Analysis Date = 07/20/14 
 Pct Recovery = 90%  Analysis Date = 07/20/14 
 Pct Recovery = 90%  Analysis Date = 07/16/14 
 Pct Recovery = 90%  Analysis Date = 07/16/14 
 Pct Recovery = 90%  Analysis Date = 07/12/14 
 Pct Recovery = 90%  Analysis Date = 07/12/14 
 Pct Recovery = 90%  Analysis Date = 07/08/14 
 Pct Recovery = 90%  Analysis Date = 07/08/14 
 Pct Recovery = 90%  Analysis Date = 07/03/14 
 Pct Recovery = 91%  Analysis Date = 07/03/14 
 Pct Recovery = 91%  Analysis Date = 06/29/14 
 Pct Recovery = 91%  Analysis Date = 06/29/14 
 Pct Recovery = 91%  Analysis Date = 06/25/14 
 Pct Recovery = 91%  Analysis Date = 06/25/14 
 Pct Recovery = 91%  Analysis Date = 06/21/14 
 Pct Recovery = 91%  Analysis Date = 06/21/14 
 Pct Recovery = 91%  Analysis Date = 06/17/14 
 Pct Recovery = 91%  Analysis Date = 06/17/14 
 Pct Recovery = 91%  Analysis Date = 06/13/14 
 Pct Recovery = 91%  Analysis Date = 06/13/14 
 Pct Recovery = 91%  Analysis Date = 06/09/14 
 Pct Recovery = 91%  Analysis Date = 06/09/14 
 Pct Recovery = 91%  Analysis Date = 06/04/14 
 Pct Recovery = 91%  Analysis Date = 06/04/14 
 Pct Recovery = 91%  Analysis Date = 05/31/14 
 Pct Recovery = 91%  Analysis Date = 05/31/14 
 Pct Recovery = 91%  Analysis Date = 05/27/14 
 Pct Recovery = 91%  Analysis Date = 05/27/14 
 Pct Recovery = 91%  Analysis Date = 05/23/14 
 Pct Recovery = 91%  Analysis Date = 05/23/14 
 Pct Recovery = 91%  Analysis Date = 05/19/14 
 Pct Recovery = 91%  Analysis Date = 05/19/14 
 Pct Recovery = 91%  Analysis Date = 05/15/14 
 Pct Recovery = 91%  Analysis Date = 05/15/14 
 Pct Recovery = 91%  Analysis Date = 05/11/14 
 Pct Recovery = 91%  Analysis Date = 05/11/14 
 Pct Recovery = 91%  Analysis Date = 05/07/14 
 Pct Recovery = 91%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
2-NITROPROPANE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 38 89% 8% 90% 8%
Total 38 89% 8% 90% 8%

Sample Statistics
2-NITROPROPANE

Characteristic N % % Basis
Plotted 38 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 38 .  
False Negatives 0 0% 0 out of 38
Not Spiked 17 .  
False Positives 0 0% 0 out of 17

BQS OBSP Determination:
2-PENTANOL, 4-METHYL-
METHOD: 4437 , TESTIDCODE: 77113GM016
Open Data Set

 Analysis Date = 07/11/14 
 SpikeMix = ChemService 2615700: 20 µl & Accu 214031128: 20 µl 
 Pct Recovery = 217%  Analysis Date = 06/07/14 
 SpikeMix = ChemService 2615700: 20 µl & Supelco LC06437: 20 µl 
 Pct Recovery = 200%  Analysis Date = 07/30/14 
 SpikeMix = NSI 031814: 10 µl & ChemService 2615700: 10 µl 
 Pct Recovery = 219%  Analysis Date = 05/20/14 
 SpikeMix = ChemService 2615700: 10 µl & Accu 214031128: 10 µl 
 Pct Recovery = 205%  Analysis Date = 07/03/14 
 SpikeMix = Abs 032014: 20 µl & ChemService 2615700: 20 µl 
 Pct Recovery = 192%  Analysis Date = 06/07/14 
 SpikeMix = ChemService 2615700: 20 µl & Supelco LC06437: 20 µl 
 Pct Recovery = 200%  Analysis Date = 06/06/14 
 SpikeMix = NSI 031814: 20 µl & ChemService 2615700: 20 µl 
 Pct Recovery = 193%  Analysis Date = 01/10/15 
 SpikeMix = Abs 032014: 20 µl & ERA 0321-14-05A: 20 µl 
 Pct Recovery = 91%  Analysis Date = 08/13/14 
 SpikeMix = ERA 0321-14-05: 20 µl & Accu 214031128: 20 µl 
 Pct Recovery = 101%  Analysis Date = 10/09/15 
 SpikeMix = Supelco LC13544: 25 µl & NSI 050515HVOC: 25 µl 
 Pct Recovery = 108%  Analysis Date = 10/09/15 
 SpikeMix = ERA 0601-15-05: 25 µl & Accu 215041338: 25 µl 
 Pct Recovery = 81%  Analysis Date = 06/26/15 
 SpikeMix = ChemService 3818700: 25 µl & Accu 215041338: 25 µl 
 Pct Recovery = 89%  Analysis Date = 08/12/16 
 SpikeMix = Accu 216041354: 15 µl & Abs 060916HVOC: 15 µl 
 Pct Recovery = 98%  Analysis Date = 04/28/16 
 SpikeMix = ChemService 3818700: 15 µl & Supelco LC13544: 15 µl 
 Pct Recovery = 97%  Analysis Date = 08/24/15 
 SpikeMix = ERA 0601-15-05: 15 µl & Supelco LC13544: 15 µl 
 Pct Recovery = 90%  Analysis Date = 07/30/15 
 SpikeMix = Supelco LC13544: 15 µl & NSI 050515HVOC: 15 µl 
 Pct Recovery = 94%  Analysis Date = 05/14/15 
 SpikeMix = ChemService 3818700: 15 µl & Supelco LC13544: 15 µl 
 Pct Recovery = 95%  Analysis Date = 11/25/15 
 SpikeMix = Accu 215041338: 15 µl & Abs 040315: 15 µl 
 Pct Recovery = 92%  Analysis Date = 09/05/15 
 SpikeMix = Accu 215041338: 15 µl & NSI 050515HVOC: 15 µl 
 Pct Recovery = 82%  Analysis Date = 11/22/14 
 SpikeMix = ChemService 2615700: 10 µl & Supelco LC06437: 10 µl 
 Pct Recovery = 176%  Analysis Date = 05/20/14 
 SpikeMix = ChemService 2615700: 10 µl & Accu 214031128: 10 µl 
 Pct Recovery = 205%  Analysis Date = 04/25/15 
 SpikeMix = Abs 032014: 10 µl & ERA 0321-14-05A: 10 µl 
 Pct Recovery = 95%  Analysis Date = 10/21/14 
 SpikeMix = ERA 0321-14-05A: 10 µl & Accu 214031128: 10 µl 
 Pct Recovery = 104%  Analysis Date = 09/06/14 
 SpikeMix = ERA 0321-14-05: 10 µl & Supelco LC06437: 10 µl 
 Pct Recovery = 117%  Analysis Date = 03/22/16 
 SpikeMix = Supelco LC13544: 10 µl & NSI 050515HVOC: 10 µl 
 Pct Recovery = 98%  Analysis Date = 12/10/15 
 SpikeMix = ChemService 3818700: 10 µl & Supelco LC13544: 10 µl 
 Pct Recovery = 92%  Analysis Date = 05/05/15 
 SpikeMix = Supelco LC13544: 10 µl & Abs 040315: 10 µl 
 Pct Recovery = 92%  Analysis Date = 02/12/16 
 SpikeMix = ERA 0601-15-05: 10 µl & Accu 215041338: 10 µl 
 Pct Recovery = 79%  Analysis Date = 01/05/16 
 SpikeMix = Accu 215041338: 10 µl & Abs 040315: 10 µl 
 Pct Recovery = 91%  Analysis Date = 05/20/15 
 SpikeMix = ChemService 3818700: 10 µl & Accu 215041338: 10 µl 
 Pct Recovery = 84%  Analysis Date = 08/12/16 
 Pct Recovery = 97%  Analysis Date = 08/07/16 
 Pct Recovery = 97%  Analysis Date = 08/07/16 
 Pct Recovery = 97%  Analysis Date = 08/03/16 
 Pct Recovery = 97%  Analysis Date = 08/03/16 
 Pct Recovery = 97%  Analysis Date = 07/30/16 
 Pct Recovery = 97%  Analysis Date = 07/30/16 
 Pct Recovery = 97%  Analysis Date = 07/26/16 
 Pct Recovery = 97%  Analysis Date = 07/26/16 
 Pct Recovery = 97%  Analysis Date = 07/22/16 
 Pct Recovery = 97%  Analysis Date = 07/22/16 
 Pct Recovery = 97%  Analysis Date = 07/18/16 
 Pct Recovery = 97%  Analysis Date = 07/18/16 
 Pct Recovery = 97%  Analysis Date = 07/14/16 
 Pct Recovery = 97%  Analysis Date = 07/14/16 
 Pct Recovery = 97%  Analysis Date = 07/10/16 
 Pct Recovery = 96%  Analysis Date = 07/10/16 
 Pct Recovery = 96%  Analysis Date = 07/06/16 
 Pct Recovery = 96%  Analysis Date = 07/06/16 
 Pct Recovery = 96%  Analysis Date = 07/02/16 
 Pct Recovery = 96%  Analysis Date = 07/02/16 
 Pct Recovery = 96%  Analysis Date = 06/28/16 
 Pct Recovery = 96%  Analysis Date = 06/28/16 
 Pct Recovery = 96%  Analysis Date = 06/24/16 
 Pct Recovery = 96%  Analysis Date = 06/24/16 
 Pct Recovery = 96%  Analysis Date = 06/20/16 
 Pct Recovery = 96%  Analysis Date = 06/20/16 
 Pct Recovery = 96%  Analysis Date = 06/15/16 
 Pct Recovery = 96%  Analysis Date = 06/15/16 
 Pct Recovery = 96%  Analysis Date = 06/11/16 
 Pct Recovery = 96%  Analysis Date = 06/11/16 
 Pct Recovery = 96%  Analysis Date = 06/07/16 
 Pct Recovery = 96%  Analysis Date = 06/07/16 
 Pct Recovery = 96%  Analysis Date = 06/03/16 
 Pct Recovery = 96%  Analysis Date = 06/03/16 
 Pct Recovery = 96%  Analysis Date = 05/30/16 
 Pct Recovery = 95%  Analysis Date = 05/30/16 
 Pct Recovery = 95%  Analysis Date = 05/26/16 
 Pct Recovery = 95%  Analysis Date = 05/26/16 
 Pct Recovery = 95%  Analysis Date = 05/22/16 
 Pct Recovery = 95%  Analysis Date = 05/22/16 
 Pct Recovery = 95%  Analysis Date = 05/18/16 
 Pct Recovery = 95%  Analysis Date = 05/18/16 
 Pct Recovery = 95%  Analysis Date = 05/14/16 
 Pct Recovery = 95%  Analysis Date = 05/14/16 
 Pct Recovery = 95%  Analysis Date = 05/10/16 
 Pct Recovery = 95%  Analysis Date = 05/10/16 
 Pct Recovery = 95%  Analysis Date = 05/06/16 
 Pct Recovery = 95%  Analysis Date = 05/06/16 
 Pct Recovery = 95%  Analysis Date = 05/02/16 
 Pct Recovery = 95%  Analysis Date = 05/02/16 
 Pct Recovery = 95%  Analysis Date = 04/28/16 
 Pct Recovery = 95%  Analysis Date = 04/28/16 
 Pct Recovery = 95%  Analysis Date = 04/23/16 
 Pct Recovery = 95%  Analysis Date = 04/23/16 
 Pct Recovery = 95%  Analysis Date = 04/19/16 
 Pct Recovery = 94%  Analysis Date = 04/19/16 
 Pct Recovery = 94%  Analysis Date = 04/15/16 
 Pct Recovery = 94%  Analysis Date = 04/15/16 
 Pct Recovery = 94%  Analysis Date = 04/11/16 
 Pct Recovery = 94%  Analysis Date = 04/11/16 
 Pct Recovery = 94%  Analysis Date = 04/07/16 
 Pct Recovery = 94%  Analysis Date = 04/07/16 
 Pct Recovery = 94%  Analysis Date = 04/03/16 
 Pct Recovery = 94%  Analysis Date = 04/03/16 
 Pct Recovery = 94%  Analysis Date = 03/30/16 
 Pct Recovery = 94%  Analysis Date = 03/30/16 
 Pct Recovery = 94%  Analysis Date = 03/26/16 
 Pct Recovery = 94%  Analysis Date = 03/26/16 
 Pct Recovery = 94%  Analysis Date = 03/22/16 
 Pct Recovery = 94%  Analysis Date = 03/22/16 
 Pct Recovery = 94%  Analysis Date = 03/18/16 
 Pct Recovery = 94%  Analysis Date = 03/18/16 
 Pct Recovery = 94%  Analysis Date = 03/14/16 
 Pct Recovery = 93%  Analysis Date = 03/14/16 
 Pct Recovery = 93%  Analysis Date = 03/10/16 
 Pct Recovery = 93%  Analysis Date = 03/10/16 
 Pct Recovery = 93%  Analysis Date = 03/06/16 
 Pct Recovery = 93%  Analysis Date = 03/06/16 
 Pct Recovery = 93%  Analysis Date = 03/02/16 
 Pct Recovery = 93%  Analysis Date = 03/02/16 
 Pct Recovery = 93%  Analysis Date = 02/26/16 
 Pct Recovery = 93%  Analysis Date = 02/26/16 
 Pct Recovery = 93%  Analysis Date = 02/22/16 
 Pct Recovery = 93%  Analysis Date = 02/22/16 
 Pct Recovery = 93%  Analysis Date = 02/18/16 
 Pct Recovery = 93%  Analysis Date = 02/18/16 
 Pct Recovery = 93%  Analysis Date = 02/14/16 
 Pct Recovery = 93%  Analysis Date = 02/14/16 
 Pct Recovery = 93%  Analysis Date = 02/10/16 
 Pct Recovery = 93%  Analysis Date = 02/10/16 
 Pct Recovery = 93%  Analysis Date = 02/06/16 
 Pct Recovery = 93%  Analysis Date = 02/06/16 
 Pct Recovery = 93%  Analysis Date = 02/02/16 
 Pct Recovery = 92%  Analysis Date = 02/02/16 
 Pct Recovery = 92%  Analysis Date = 01/29/16 
 Pct Recovery = 92%  Analysis Date = 01/29/16 
 Pct Recovery = 92%  Analysis Date = 01/25/16 
 Pct Recovery = 92%  Analysis Date = 01/25/16 
 Pct Recovery = 92%  Analysis Date = 01/21/16 
 Pct Recovery = 92%  Analysis Date = 01/21/16 
 Pct Recovery = 92%  Analysis Date = 01/17/16 
 Pct Recovery = 92%  Analysis Date = 01/17/16 
 Pct Recovery = 92%  Analysis Date = 01/13/16 
 Pct Recovery = 92%  Analysis Date = 01/13/16 
 Pct Recovery = 92%  Analysis Date = 01/09/16 
 Pct Recovery = 92%  Analysis Date = 01/09/16 
 Pct Recovery = 92%  Analysis Date = 01/04/16 
 Pct Recovery = 92%  Analysis Date = 01/04/16 
 Pct Recovery = 92%  Analysis Date = 12/31/15 
 Pct Recovery = 92%  Analysis Date = 12/31/15 
 Pct Recovery = 92%  Analysis Date = 12/27/15 
 Pct Recovery = 92%  Analysis Date = 12/27/15 
 Pct Recovery = 92%  Analysis Date = 12/23/15 
 Pct Recovery = 91%  Analysis Date = 12/23/15 
 Pct Recovery = 91%  Analysis Date = 12/19/15 
 Pct Recovery = 91%  Analysis Date = 12/19/15 
 Pct Recovery = 91%  Analysis Date = 12/15/15 
 Pct Recovery = 91%  Analysis Date = 12/15/15 
 Pct Recovery = 91%  Analysis Date = 12/11/15 
 Pct Recovery = 91%  Analysis Date = 12/11/15 
 Pct Recovery = 91%  Analysis Date = 12/07/15 
 Pct Recovery = 91%  Analysis Date = 12/07/15 
 Pct Recovery = 91%  Analysis Date = 12/03/15 
 Pct Recovery = 91%  Analysis Date = 12/03/15 
 Pct Recovery = 91%  Analysis Date = 11/29/15 
 Pct Recovery = 91%  Analysis Date = 11/29/15 
 Pct Recovery = 91%  Analysis Date = 11/25/15 
 Pct Recovery = 91%  Analysis Date = 11/25/15 
 Pct Recovery = 91%  Analysis Date = 11/21/15 
 Pct Recovery = 91%  Analysis Date = 11/21/15 
 Pct Recovery = 91%  Analysis Date = 11/17/15 
 Pct Recovery = 91%  Analysis Date = 11/17/15 
 Pct Recovery = 91%  Analysis Date = 11/12/15 
 Pct Recovery = 91%  Analysis Date = 11/12/15 
 Pct Recovery = 91%  Analysis Date = 11/08/15 
 Pct Recovery = 91%  Analysis Date = 11/08/15 
 Pct Recovery = 91%  Analysis Date = 11/04/15 
 Pct Recovery = 91%  Analysis Date = 11/04/15 
 Pct Recovery = 91%  Analysis Date = 10/31/15 
 Pct Recovery = 91%  Analysis Date = 10/31/15 
 Pct Recovery = 91%  Analysis Date = 10/27/15 
 Pct Recovery = 91%  Analysis Date = 10/27/15 
 Pct Recovery = 91%  Analysis Date = 10/23/15 
 Pct Recovery = 91%  Analysis Date = 10/23/15 
 Pct Recovery = 91%  Analysis Date = 10/19/15 
 Pct Recovery = 91%  Analysis Date = 10/19/15 
 Pct Recovery = 91%  Analysis Date = 10/15/15 
 Pct Recovery = 91%  Analysis Date = 10/15/15 
 Pct Recovery = 91%  Analysis Date = 10/11/15 
 Pct Recovery = 91%  Analysis Date = 10/11/15 
 Pct Recovery = 91%  Analysis Date = 10/07/15 
 Pct Recovery = 91%  Analysis Date = 10/07/15 
 Pct Recovery = 91%  Analysis Date = 10/03/15 
 Pct Recovery = 91%  Analysis Date = 10/03/15 
 Pct Recovery = 91%  Analysis Date = 09/29/15 
 Pct Recovery = 91%  Analysis Date = 09/29/15 
 Pct Recovery = 91%  Analysis Date = 09/25/15 
 Pct Recovery = 91%  Analysis Date = 09/25/15 
 Pct Recovery = 91%  Analysis Date = 09/21/15 
 Pct Recovery = 91%  Analysis Date = 09/21/15 
 Pct Recovery = 91%  Analysis Date = 09/16/15 
 Pct Recovery = 91%  Analysis Date = 09/16/15 
 Pct Recovery = 91%  Analysis Date = 09/12/15 
 Pct Recovery = 91%  Analysis Date = 09/12/15 
 Pct Recovery = 91%  Analysis Date = 09/08/15 
 Pct Recovery = 91%  Analysis Date = 09/08/15 
 Pct Recovery = 91%  Analysis Date = 09/04/15 
 Pct Recovery = 91%  Analysis Date = 09/04/15 
 Pct Recovery = 91%  Analysis Date = 08/31/15 
 Pct Recovery = 91%  Analysis Date = 08/31/15 
 Pct Recovery = 91%  Analysis Date = 08/27/15 
 Pct Recovery = 91%  Analysis Date = 08/27/15 
 Pct Recovery = 91%  Analysis Date = 08/23/15 
 Pct Recovery = 91%  Analysis Date = 08/23/15 
 Pct Recovery = 91%  Analysis Date = 08/19/15 
 Pct Recovery = 91%  Analysis Date = 08/19/15 
 Pct Recovery = 91%  Analysis Date = 08/15/15 
 Pct Recovery = 91%  Analysis Date = 08/15/15 
 Pct Recovery = 91%  Analysis Date = 08/11/15 
 Pct Recovery = 91%  Analysis Date = 08/11/15 
 Pct Recovery = 91%  Analysis Date = 08/07/15 
 Pct Recovery = 91%  Analysis Date = 08/07/15 
 Pct Recovery = 91%  Analysis Date = 08/03/15 
 Pct Recovery = 91%  Analysis Date = 08/03/15 
 Pct Recovery = 91%  Analysis Date = 07/30/15 
 Pct Recovery = 91%  Analysis Date = 07/30/15 
 Pct Recovery = 91%  Analysis Date = 07/25/15 
 Pct Recovery = 91%  Analysis Date = 07/25/15 
 Pct Recovery = 91%  Analysis Date = 07/21/15 
 Pct Recovery = 91%  Analysis Date = 07/21/15 
 Pct Recovery = 91%  Analysis Date = 07/17/15 
 Pct Recovery = 91%  Analysis Date = 07/17/15 
 Pct Recovery = 91%  Analysis Date = 07/13/15 
 Pct Recovery = 91%  Analysis Date = 07/13/15 
 Pct Recovery = 91%  Analysis Date = 07/09/15 
 Pct Recovery = 91%  Analysis Date = 07/09/15 
 Pct Recovery = 91%  Analysis Date = 07/05/15 
 Pct Recovery = 91%  Analysis Date = 07/05/15 
 Pct Recovery = 91%  Analysis Date = 07/01/15 
 Pct Recovery = 91%  Analysis Date = 07/01/15 
 Pct Recovery = 91%  Analysis Date = 06/27/15 
 Pct Recovery = 91%  Analysis Date = 06/27/15 
 Pct Recovery = 91%  Analysis Date = 06/23/15 
 Pct Recovery = 91%  Analysis Date = 06/23/15 
 Pct Recovery = 91%  Analysis Date = 06/19/15 
 Pct Recovery = 92%  Analysis Date = 06/19/15 
 Pct Recovery = 92%  Analysis Date = 06/15/15 
 Pct Recovery = 92%  Analysis Date = 06/15/15 
 Pct Recovery = 92%  Analysis Date = 06/11/15 
 Pct Recovery = 92%  Analysis Date = 06/11/15 
 Pct Recovery = 92%  Analysis Date = 06/07/15 
 Pct Recovery = 93%  Analysis Date = 06/07/15 
 Pct Recovery = 93%  Analysis Date = 06/02/15 
 Pct Recovery = 93%  Analysis Date = 06/02/15 
 Pct Recovery = 93%  Analysis Date = 05/29/15 
 Pct Recovery = 94%  Analysis Date = 05/29/15 
 Pct Recovery = 94%  Analysis Date = 05/25/15 
 Pct Recovery = 94%  Analysis Date = 05/25/15 
 Pct Recovery = 94%  Analysis Date = 05/21/15 
 Pct Recovery = 94%  Analysis Date = 05/21/15 
 Pct Recovery = 94%  Analysis Date = 05/17/15 
 Pct Recovery = 95%  Analysis Date = 05/17/15 
 Pct Recovery = 95%  Analysis Date = 05/13/15 
 Pct Recovery = 95%  Analysis Date = 05/13/15 
 Pct Recovery = 95%  Analysis Date = 05/09/15 
 Pct Recovery = 96%  Analysis Date = 05/09/15 
 Pct Recovery = 96%  Analysis Date = 05/05/15 
 Pct Recovery = 96%  Analysis Date = 05/05/15 
 Pct Recovery = 96%  Analysis Date = 05/01/15 
 Pct Recovery = 97%  Analysis Date = 05/01/15 
 Pct Recovery = 97%  Analysis Date = 04/27/15 
 Pct Recovery = 98%  Analysis Date = 04/27/15 
 Pct Recovery = 98%  Analysis Date = 04/23/15 
 Pct Recovery = 98%  Analysis Date = 04/23/15 
 Pct Recovery = 98%  Analysis Date = 04/19/15 
 Pct Recovery = 99%  Analysis Date = 04/19/15 
 Pct Recovery = 99%  Analysis Date = 04/15/15 
 Pct Recovery = 100%  Analysis Date = 04/15/15 
 Pct Recovery = 100%  Analysis Date = 04/11/15 
 Pct Recovery = 100%  Analysis Date = 04/11/15 
 Pct Recovery = 100%  Analysis Date = 04/06/15 
 Pct Recovery = 101%  Analysis Date = 04/06/15 
 Pct Recovery = 101%  Analysis Date = 04/02/15 
 Pct Recovery = 102%  Analysis Date = 04/02/15 
 Pct Recovery = 102%  Analysis Date = 03/29/15 
 Pct Recovery = 102%  Analysis Date = 03/29/15 
 Pct Recovery = 102%  Analysis Date = 03/25/15 
 Pct Recovery = 103%  Analysis Date = 03/25/15 
 Pct Recovery = 103%  Analysis Date = 03/21/15 
 Pct Recovery = 104%  Analysis Date = 03/21/15 
 Pct Recovery = 104%  Analysis Date = 03/17/15 
 Pct Recovery = 104%  Analysis Date = 03/17/15 
 Pct Recovery = 104%  Analysis Date = 03/13/15 
 Pct Recovery = 105%  Analysis Date = 03/13/15 
 Pct Recovery = 105%  Analysis Date = 03/09/15 
 Pct Recovery = 106%  Analysis Date = 03/09/15 
 Pct Recovery = 106%  Analysis Date = 03/05/15 
 Pct Recovery = 106%  Analysis Date = 03/05/15 
 Pct Recovery = 106%  Analysis Date = 03/01/15 
 Pct Recovery = 107%  Analysis Date = 03/01/15 
 Pct Recovery = 107%  Analysis Date = 02/25/15 
 Pct Recovery = 107%  Analysis Date = 02/25/15 
 Pct Recovery = 107%  Analysis Date = 02/21/15 
 Pct Recovery = 108%  Analysis Date = 02/21/15 
 Pct Recovery = 108%  Analysis Date = 02/17/15 
 Pct Recovery = 109%  Analysis Date = 02/17/15 
 Pct Recovery = 109%  Analysis Date = 02/12/15 
 Pct Recovery = 109%  Analysis Date = 02/12/15 
 Pct Recovery = 109%  Analysis Date = 02/08/15 
 Pct Recovery = 110%  Analysis Date = 02/08/15 
 Pct Recovery = 110%  Analysis Date = 02/04/15 
 Pct Recovery = 111%  Analysis Date = 02/04/15 
 Pct Recovery = 111%  Analysis Date = 01/31/15 
 Pct Recovery = 111%  Analysis Date = 01/31/15 
 Pct Recovery = 111%  Analysis Date = 01/27/15 
 Pct Recovery = 112%  Analysis Date = 01/27/15 
 Pct Recovery = 112%  Analysis Date = 01/23/15 
 Pct Recovery = 113%  Analysis Date = 01/23/15 
 Pct Recovery = 113%  Analysis Date = 01/19/15 
 Pct Recovery = 113%  Analysis Date = 01/19/15 
 Pct Recovery = 113%  Analysis Date = 01/15/15 
 Pct Recovery = 114%  Analysis Date = 01/15/15 
 Pct Recovery = 114%  Analysis Date = 01/11/15 
 Pct Recovery = 115%  Analysis Date = 01/11/15 
 Pct Recovery = 115%  Analysis Date = 01/07/15 
 Pct Recovery = 116%  Analysis Date = 01/07/15 
 Pct Recovery = 116%  Analysis Date = 01/03/15 
 Pct Recovery = 117%  Analysis Date = 01/03/15 
 Pct Recovery = 117%  Analysis Date = 12/30/14 
 Pct Recovery = 118%  Analysis Date = 12/30/14 
 Pct Recovery = 118%  Analysis Date = 12/26/14 
 Pct Recovery = 119%  Analysis Date = 12/26/14 
 Pct Recovery = 119%  Analysis Date = 12/21/14 
 Pct Recovery = 121%  Analysis Date = 12/21/14 
 Pct Recovery = 121%  Analysis Date = 12/17/14 
 Pct Recovery = 122%  Analysis Date = 12/17/14 
 Pct Recovery = 122%  Analysis Date = 12/13/14 
 Pct Recovery = 123%  Analysis Date = 12/13/14 
 Pct Recovery = 123%  Analysis Date = 12/09/14 
 Pct Recovery = 124%  Analysis Date = 12/09/14 
 Pct Recovery = 124%  Analysis Date = 12/05/14 
 Pct Recovery = 126%  Analysis Date = 12/05/14 
 Pct Recovery = 126%  Analysis Date = 12/01/14 
 Pct Recovery = 127%  Analysis Date = 12/01/14 
 Pct Recovery = 127%  Analysis Date = 11/27/14 
 Pct Recovery = 128%  Analysis Date = 11/27/14 
 Pct Recovery = 128%  Analysis Date = 11/23/14 
 Pct Recovery = 129%  Analysis Date = 11/23/14 
 Pct Recovery = 129%  Analysis Date = 11/19/14 
 Pct Recovery = 131%  Analysis Date = 11/19/14 
 Pct Recovery = 131%  Analysis Date = 11/15/14 
 Pct Recovery = 132%  Analysis Date = 11/15/14 
 Pct Recovery = 132%  Analysis Date = 11/11/14 
 Pct Recovery = 133%  Analysis Date = 11/11/14 
 Pct Recovery = 133%  Analysis Date = 11/07/14 
 Pct Recovery = 134%  Analysis Date = 11/07/14 
 Pct Recovery = 134%  Analysis Date = 11/03/14 
 Pct Recovery = 136%  Analysis Date = 11/03/14 
 Pct Recovery = 136%  Analysis Date = 10/30/14 
 Pct Recovery = 137%  Analysis Date = 10/30/14 
 Pct Recovery = 137%  Analysis Date = 10/25/14 
 Pct Recovery = 138%  Analysis Date = 10/25/14 
 Pct Recovery = 138%  Analysis Date = 10/21/14 
 Pct Recovery = 139%  Analysis Date = 10/21/14 
 Pct Recovery = 139%  Analysis Date = 10/17/14 
 Pct Recovery = 141%  Analysis Date = 10/17/14 
 Pct Recovery = 141%  Analysis Date = 10/13/14 
 Pct Recovery = 143%  Analysis Date = 10/13/14 
 Pct Recovery = 143%  Analysis Date = 10/09/14 
 Pct Recovery = 144%  Analysis Date = 10/09/14 
 Pct Recovery = 144%  Analysis Date = 10/05/14 
 Pct Recovery = 146%  Analysis Date = 10/05/14 
 Pct Recovery = 146%  Analysis Date = 10/01/14 
 Pct Recovery = 147%  Analysis Date = 10/01/14 
 Pct Recovery = 147%  Analysis Date = 09/27/14 
 Pct Recovery = 149%  Analysis Date = 09/27/14 
 Pct Recovery = 149%  Analysis Date = 09/23/14 
 Pct Recovery = 151%  Analysis Date = 09/23/14 
 Pct Recovery = 151%  Analysis Date = 09/19/14 
 Pct Recovery = 152%  Analysis Date = 09/19/14 
 Pct Recovery = 152%  Analysis Date = 09/15/14 
 Pct Recovery = 154%  Analysis Date = 09/15/14 
 Pct Recovery = 154%  Analysis Date = 09/11/14 
 Pct Recovery = 156%  Analysis Date = 09/11/14 
 Pct Recovery = 156%  Analysis Date = 09/07/14 
 Pct Recovery = 157%  Analysis Date = 09/07/14 
 Pct Recovery = 157%  Analysis Date = 09/02/14 
 Pct Recovery = 159%  Analysis Date = 09/02/14 
 Pct Recovery = 159%  Analysis Date = 08/29/14 
 Pct Recovery = 161%  Analysis Date = 08/29/14 
 Pct Recovery = 161%  Analysis Date = 08/25/14 
 Pct Recovery = 162%  Analysis Date = 08/25/14 
 Pct Recovery = 162%  Analysis Date = 08/21/14 
 Pct Recovery = 164%  Analysis Date = 08/21/14 
 Pct Recovery = 164%  Analysis Date = 08/17/14 
 Pct Recovery = 165%  Analysis Date = 08/17/14 
 Pct Recovery = 165%  Analysis Date = 08/13/14 
 Pct Recovery = 167%  Analysis Date = 08/13/14 
 Pct Recovery = 167%  Analysis Date = 08/09/14 
 Pct Recovery = 169%  Analysis Date = 08/09/14 
 Pct Recovery = 169%  Analysis Date = 08/05/14 
 Pct Recovery = 171%  Analysis Date = 08/05/14 
 Pct Recovery = 171%  Analysis Date = 08/01/14 
 Pct Recovery = 172%  Analysis Date = 08/01/14 
 Pct Recovery = 172%  Analysis Date = 07/28/14 
 Pct Recovery = 174%  Analysis Date = 07/28/14 
 Pct Recovery = 174%  Analysis Date = 07/24/14 
 Pct Recovery = 176%  Analysis Date = 07/24/14 
 Pct Recovery = 176%  Analysis Date = 07/20/14 
 Pct Recovery = 178%  Analysis Date = 07/20/14 
 Pct Recovery = 178%  Analysis Date = 07/16/14 
 Pct Recovery = 179%  Analysis Date = 07/16/14 
 Pct Recovery = 179%  Analysis Date = 07/11/14 
 Pct Recovery = 181%  Analysis Date = 07/11/14 
 Pct Recovery = 181%  Analysis Date = 07/07/14 
 Pct Recovery = 183%  Analysis Date = 07/07/14 
 Pct Recovery = 183%  Analysis Date = 07/03/14 
 Pct Recovery = 184%  Analysis Date = 07/03/14 
 Pct Recovery = 184%  Analysis Date = 06/29/14 
 Pct Recovery = 186%  Analysis Date = 06/29/14 
 Pct Recovery = 186%  Analysis Date = 06/25/14 
 Pct Recovery = 188%  Analysis Date = 06/25/14 
 Pct Recovery = 188%  Analysis Date = 06/21/14 
 Pct Recovery = 190%  Analysis Date = 06/21/14 
 Pct Recovery = 190%  Analysis Date = 06/17/14 
 Pct Recovery = 192%  Analysis Date = 06/17/14 
 Pct Recovery = 192%  Analysis Date = 06/13/14 
 Pct Recovery = 194%  Analysis Date = 06/13/14 
 Pct Recovery = 194%  Analysis Date = 06/09/14 
 Pct Recovery = 195%  Analysis Date = 06/09/14 
 Pct Recovery = 195%  Analysis Date = 06/05/14 
 Pct Recovery = 197%  Analysis Date = 06/05/14 
 Pct Recovery = 197%  Analysis Date = 06/01/14 
 Pct Recovery = 199%  Analysis Date = 06/01/14 
 Pct Recovery = 199%  Analysis Date = 05/28/14 
 Pct Recovery = 201%  Analysis Date = 05/28/14 
 Pct Recovery = 201%  Analysis Date = 05/24/14 
 Pct Recovery = 203%  Analysis Date = 05/24/14 
 Pct Recovery = 203%  Analysis Date = 05/20/14 
 Pct Recovery = 205%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
2-PENTANOL, 4-METHYL-

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 28 121% 48% 96% 41%
Total 28 121% 48% 96% 41%

Sample Statistics
2-PENTANOL, 4-METHYL-

Characteristic N % % Basis
Plotted 28 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 28 .  
False Negatives 0 0% 0 out of 28
Not Spiked 20 .  
False Positives 0 0% 0 out of 20

BQS OBSP Determination:
2-PROPEN-1-OL
METHOD: 4437 , TESTIDCODE: 68729GM016
Open Data Set

 Analysis Date = 07/29/16 
 SpikeMix = Supelco LC20145V: 40 µl & NSI 041516: 40 µl & NSI 041416HVOC: 40 µl 
 Pct Recovery = 88%  Analysis Date = 07/06/16 
 SpikeMix = Accu 216041354: 40 µl & NSI 041516: 40 µl & NSI 041416HVOC: 40 µl 
 Pct Recovery = 98%  Analysis Date = 06/29/16 
 SpikeMix = NSI 041516: 40 µl & ChemService 5082800: 40 µl 
 Pct Recovery = 99%  Analysis Date = 07/14/16 
 SpikeMix = NSI 041516: 25 µl & ChemService 5082800: 25 µl & NSI 041416HVOC: 25 µl 
 Pct Recovery = 82%  Analysis Date = 05/21/16 
 SpikeMix = Supelco LC20145V: 25 µl & NSI 041516: 25 µl & NSI 041416HVOC: 25 µl 
 Pct Recovery = 87%  Analysis Date = 10/09/15 
 SpikeMix = Supelco LC13544: 25 µl & NSI 050515HVOC: 25 µl 
 Pct Recovery = 96%  Analysis Date = 10/09/15 
 SpikeMix = ERA 0601-15-05: 25 µl & Accu 215041338: 25 µl 
 Pct Recovery = 93%  Analysis Date = 06/26/15 
 SpikeMix = ChemService 3818700: 25 µl & Accu 215041338: 25 µl 
 Pct Recovery = 95%  Analysis Date = 08/12/16 
 SpikeMix = Accu 216041354: 15 µl & Abs 060916HVOC: 15 µl 
 Pct Recovery = 92%  Analysis Date = 06/03/16 
 SpikeMix = NSI 041516: 15 µl & Phenova B20160303: 15 µl & NSI 041416HVOC: 15 µl 
 Pct Recovery = 94%  Analysis Date = 05/20/16 
 SpikeMix = Accu 216041354: 15 µl & NSI 041516: 15 µl & Accu 216041225: 15 µl 
 Pct Recovery = 79%  Analysis Date = 04/28/16 
 SpikeMix = ChemService 3818700: 15 µl & Supelco LC13544: 15 µl 
 Pct Recovery = 94%  Analysis Date = 08/24/15 
 SpikeMix = ERA 0601-15-05: 15 µl & Supelco LC13544: 15 µl 
 Pct Recovery = 101%  Analysis Date = 07/30/15 
 SpikeMix = Supelco LC13544: 15 µl & NSI 050515HVOC: 15 µl 
 Pct Recovery = 91%  Analysis Date = 05/14/15 
 SpikeMix = ChemService 3818700: 15 µl & Supelco LC13544: 15 µl 
 Pct Recovery = 99%  Analysis Date = 11/25/15 
 SpikeMix = Accu 215041338: 15 µl & Abs 040315: 15 µl 
 Pct Recovery = 87%  Analysis Date = 09/05/15 
 SpikeMix = Accu 215041338: 15 µl & NSI 050515HVOC: 15 µl 
 Pct Recovery = 86%  Analysis Date = 03/22/16 
 SpikeMix = Supelco LC13544: 10 µl & NSI 050515HVOC: 10 µl 
 Pct Recovery = 85%  Analysis Date = 12/10/15 
 SpikeMix = ChemService 3818700: 10 µl & Supelco LC13544: 10 µl 
 Pct Recovery = 92%  Analysis Date = 05/05/15 
 SpikeMix = Supelco LC13544: 10 µl & Abs 040315: 10 µl 
 Pct Recovery = 91%  Analysis Date = 02/12/16 
 SpikeMix = ERA 0601-15-05: 10 µl & Accu 215041338: 10 µl 
 Pct Recovery = 93%  Analysis Date = 01/05/16 
 SpikeMix = Accu 215041338: 10 µl & Abs 040315: 10 µl 
 Pct Recovery = 96%  Analysis Date = 05/20/15 
 SpikeMix = ChemService 3818700: 10 µl & Accu 215041338: 10 µl 
 Pct Recovery = 101%  Analysis Date = 08/20/14 
 SpikeMix = Supelco LC06437: 20 µl & Abs 032014: 20 µl 
 Pct Recovery = 136%  Analysis Date = 07/23/14 
 SpikeMix = Accu 214031128: 20 µl & Abs 032014: 20 µl 
 Pct Recovery = 96%  Analysis Date = 07/03/14 
 SpikeMix = Abs 032014: 20 µl & ChemService 2615700: 20 µl 
 Pct Recovery = 99%  Analysis Date = 06/06/14 
 SpikeMix = NSI 031814: 20 µl & ChemService 2615700: 20 µl 
 Pct Recovery = 106%  Analysis Date = 05/07/14 
 SpikeMix = NSI 031814: 20 µl & Accu 214031128: 20 µl 
 Pct Recovery = 75%  Analysis Date = 01/10/15 
 SpikeMix = Abs 032014: 20 µl & ERA 0321-14-05A: 20 µl 
 Pct Recovery = 101%  Analysis Date = 03/19/15 
 SpikeMix = Supelco LC06437: 20 µl & NSI 031814: 20 µl 
 Pct Recovery = 98%  Analysis Date = 08/11/16 
 Pct Recovery = 90%  Analysis Date = 08/07/16 
 Pct Recovery = 90%  Analysis Date = 08/07/16 
 Pct Recovery = 90%  Analysis Date = 08/03/16 
 Pct Recovery = 90%  Analysis Date = 08/03/16 
 Pct Recovery = 90%  Analysis Date = 07/30/16 
 Pct Recovery = 90%  Analysis Date = 07/30/16 
 Pct Recovery = 90%  Analysis Date = 07/26/16 
 Pct Recovery = 90%  Analysis Date = 07/26/16 
 Pct Recovery = 90%  Analysis Date = 07/22/16 
 Pct Recovery = 90%  Analysis Date = 07/22/16 
 Pct Recovery = 90%  Analysis Date = 07/18/16 
 Pct Recovery = 90%  Analysis Date = 07/18/16 
 Pct Recovery = 90%  Analysis Date = 07/14/16 
 Pct Recovery = 90%  Analysis Date = 07/14/16 
 Pct Recovery = 90%  Analysis Date = 07/09/16 
 Pct Recovery = 90%  Analysis Date = 07/09/16 
 Pct Recovery = 90%  Analysis Date = 07/05/16 
 Pct Recovery = 90%  Analysis Date = 07/05/16 
 Pct Recovery = 90%  Analysis Date = 07/01/16 
 Pct Recovery = 90%  Analysis Date = 07/01/16 
 Pct Recovery = 90%  Analysis Date = 06/27/16 
 Pct Recovery = 90%  Analysis Date = 06/27/16 
 Pct Recovery = 90%  Analysis Date = 06/23/16 
 Pct Recovery = 90%  Analysis Date = 06/23/16 
 Pct Recovery = 90%  Analysis Date = 06/19/16 
 Pct Recovery = 90%  Analysis Date = 06/19/16 
 Pct Recovery = 90%  Analysis Date = 06/15/16 
 Pct Recovery = 90%  Analysis Date = 06/15/16 
 Pct Recovery = 90%  Analysis Date = 06/10/16 
 Pct Recovery = 90%  Analysis Date = 06/10/16 
 Pct Recovery = 90%  Analysis Date = 06/06/16 
 Pct Recovery = 90%  Analysis Date = 06/06/16 
 Pct Recovery = 90%  Analysis Date = 06/02/16 
 Pct Recovery = 90%  Analysis Date = 06/02/16 
 Pct Recovery = 90%  Analysis Date = 05/29/16 
 Pct Recovery = 90%  Analysis Date = 05/29/16 
 Pct Recovery = 90%  Analysis Date = 05/25/16 
 Pct Recovery = 90%  Analysis Date = 05/25/16 
 Pct Recovery = 90%  Analysis Date = 05/21/16 
 Pct Recovery = 90%  Analysis Date = 05/21/16 
 Pct Recovery = 90%  Analysis Date = 05/17/16 
 Pct Recovery = 90%  Analysis Date = 05/17/16 
 Pct Recovery = 90%  Analysis Date = 05/12/16 
 Pct Recovery = 90%  Analysis Date = 05/12/16 
 Pct Recovery = 90%  Analysis Date = 05/08/16 
 Pct Recovery = 90%  Analysis Date = 05/08/16 
 Pct Recovery = 90%  Analysis Date = 05/04/16 
 Pct Recovery = 90%  Analysis Date = 05/04/16 
 Pct Recovery = 90%  Analysis Date = 04/30/16 
 Pct Recovery = 90%  Analysis Date = 04/30/16 
 Pct Recovery = 90%  Analysis Date = 04/26/16 
 Pct Recovery = 91%  Analysis Date = 04/26/16 
 Pct Recovery = 91%  Analysis Date = 04/22/16 
 Pct Recovery = 91%  Analysis Date = 04/22/16 
 Pct Recovery = 91%  Analysis Date = 04/18/16 
 Pct Recovery = 91%  Analysis Date = 04/18/16 
 Pct Recovery = 91%  Analysis Date = 04/13/16 
 Pct Recovery = 91%  Analysis Date = 04/13/16 
 Pct Recovery = 91%  Analysis Date = 04/09/16 
 Pct Recovery = 91%  Analysis Date = 04/09/16 
 Pct Recovery = 91%  Analysis Date = 04/05/16 
 Pct Recovery = 91%  Analysis Date = 04/05/16 
 Pct Recovery = 91%  Analysis Date = 04/01/16 
 Pct Recovery = 91%  Analysis Date = 04/01/16 
 Pct Recovery = 91%  Analysis Date = 03/28/16 
 Pct Recovery = 91%  Analysis Date = 03/28/16 
 Pct Recovery = 91%  Analysis Date = 03/24/16 
 Pct Recovery = 91%  Analysis Date = 03/24/16 
 Pct Recovery = 91%  Analysis Date = 03/20/16 
 Pct Recovery = 91%  Analysis Date = 03/20/16 
 Pct Recovery = 91%  Analysis Date = 03/15/16 
 Pct Recovery = 91%  Analysis Date = 03/15/16 
 Pct Recovery = 91%  Analysis Date = 03/11/16 
 Pct Recovery = 91%  Analysis Date = 03/11/16 
 Pct Recovery = 91%  Analysis Date = 03/07/16 
 Pct Recovery = 91%  Analysis Date = 03/07/16 
 Pct Recovery = 91%  Analysis Date = 03/03/16 
 Pct Recovery = 91%  Analysis Date = 03/03/16 
 Pct Recovery = 91%  Analysis Date = 02/28/16 
 Pct Recovery = 91%  Analysis Date = 02/28/16 
 Pct Recovery = 91%  Analysis Date = 02/24/16 
 Pct Recovery = 91%  Analysis Date = 02/24/16 
 Pct Recovery = 91%  Analysis Date = 02/20/16 
 Pct Recovery = 91%  Analysis Date = 02/20/16 
 Pct Recovery = 91%  Analysis Date = 02/15/16 
 Pct Recovery = 91%  Analysis Date = 02/15/16 
 Pct Recovery = 91%  Analysis Date = 02/11/16 
 Pct Recovery = 91%  Analysis Date = 02/11/16 
 Pct Recovery = 91%  Analysis Date = 02/07/16 
 Pct Recovery = 91%  Analysis Date = 02/07/16 
 Pct Recovery = 91%  Analysis Date = 02/03/16 
 Pct Recovery = 91%  Analysis Date = 02/03/16 
 Pct Recovery = 91%  Analysis Date = 01/30/16 
 Pct Recovery = 91%  Analysis Date = 01/30/16 
 Pct Recovery = 91%  Analysis Date = 01/26/16 
 Pct Recovery = 91%  Analysis Date = 01/26/16 
 Pct Recovery = 91%  Analysis Date = 01/22/16 
 Pct Recovery = 91%  Analysis Date = 01/22/16 
 Pct Recovery = 91%  Analysis Date = 01/17/16 
 Pct Recovery = 91%  Analysis Date = 01/17/16 
 Pct Recovery = 91%  Analysis Date = 01/13/16 
 Pct Recovery = 91%  Analysis Date = 01/13/16 
 Pct Recovery = 91%  Analysis Date = 01/09/16 
 Pct Recovery = 91%  Analysis Date = 01/09/16 
 Pct Recovery = 91%  Analysis Date = 01/05/16 
 Pct Recovery = 91%  Analysis Date = 01/05/16 
 Pct Recovery = 91%  Analysis Date = 01/01/16 
 Pct Recovery = 91%  Analysis Date = 01/01/16 
 Pct Recovery = 91%  Analysis Date = 12/28/15 
 Pct Recovery = 91%  Analysis Date = 12/28/15 
 Pct Recovery = 91%  Analysis Date = 12/24/15 
 Pct Recovery = 92%  Analysis Date = 12/24/15 
 Pct Recovery = 92%  Analysis Date = 12/20/15 
 Pct Recovery = 92%  Analysis Date = 12/20/15 
 Pct Recovery = 92%  Analysis Date = 12/15/15 
 Pct Recovery = 92%  Analysis Date = 12/15/15 
 Pct Recovery = 92%  Analysis Date = 12/11/15 
 Pct Recovery = 92%  Analysis Date = 12/11/15 
 Pct Recovery = 92%  Analysis Date = 12/07/15 
 Pct Recovery = 92%  Analysis Date = 12/07/15 
 Pct Recovery = 92%  Analysis Date = 12/03/15 
 Pct Recovery = 92%  Analysis Date = 12/03/15 
 Pct Recovery = 92%  Analysis Date = 11/29/15 
 Pct Recovery = 92%  Analysis Date = 11/29/15 
 Pct Recovery = 92%  Analysis Date = 11/25/15 
 Pct Recovery = 92%  Analysis Date = 11/25/15 
 Pct Recovery = 92%  Analysis Date = 11/21/15 
 Pct Recovery = 92%  Analysis Date = 11/21/15 
 Pct Recovery = 92%  Analysis Date = 11/16/15 
 Pct Recovery = 92%  Analysis Date = 11/16/15 
 Pct Recovery = 92%  Analysis Date = 11/12/15 
 Pct Recovery = 92%  Analysis Date = 11/12/15 
 Pct Recovery = 92%  Analysis Date = 11/08/15 
 Pct Recovery = 92%  Analysis Date = 11/08/15 
 Pct Recovery = 92%  Analysis Date = 11/04/15 
 Pct Recovery = 93%  Analysis Date = 11/04/15 
 Pct Recovery = 93%  Analysis Date = 10/31/15 
 Pct Recovery = 93%  Analysis Date = 10/31/15 
 Pct Recovery = 93%  Analysis Date = 10/27/15 
 Pct Recovery = 93%  Analysis Date = 10/27/15 
 Pct Recovery = 93%  Analysis Date = 10/23/15 
 Pct Recovery = 93%  Analysis Date = 10/23/15 
 Pct Recovery = 93%  Analysis Date = 10/18/15 
 Pct Recovery = 93%  Analysis Date = 10/18/15 
 Pct Recovery = 93%  Analysis Date = 10/14/15 
 Pct Recovery = 93%  Analysis Date = 10/14/15 
 Pct Recovery = 93%  Analysis Date = 10/10/15 
 Pct Recovery = 93%  Analysis Date = 10/10/15 
 Pct Recovery = 93%  Analysis Date = 10/06/15 
 Pct Recovery = 93%  Analysis Date = 10/06/15 
 Pct Recovery = 93%  Analysis Date = 10/02/15 
 Pct Recovery = 93%  Analysis Date = 10/02/15 
 Pct Recovery = 93%  Analysis Date = 09/28/15 
 Pct Recovery = 93%  Analysis Date = 09/28/15 
 Pct Recovery = 93%  Analysis Date = 09/24/15 
 Pct Recovery = 93%  Analysis Date = 09/24/15 
 Pct Recovery = 93%  Analysis Date = 09/19/15 
 Pct Recovery = 94%  Analysis Date = 09/19/15 
 Pct Recovery = 94%  Analysis Date = 09/15/15 
 Pct Recovery = 94%  Analysis Date = 09/15/15 
 Pct Recovery = 94%  Analysis Date = 09/11/15 
 Pct Recovery = 94%  Analysis Date = 09/11/15 
 Pct Recovery = 94%  Analysis Date = 09/07/15 
 Pct Recovery = 94%  Analysis Date = 09/07/15 
 Pct Recovery = 94%  Analysis Date = 09/03/15 
 Pct Recovery = 94%  Analysis Date = 09/03/15 
 Pct Recovery = 94%  Analysis Date = 08/30/15 
 Pct Recovery = 94%  Analysis Date = 08/30/15 
 Pct Recovery = 94%  Analysis Date = 08/26/15 
 Pct Recovery = 94%  Analysis Date = 08/26/15 
 Pct Recovery = 94%  Analysis Date = 08/21/15 
 Pct Recovery = 94%  Analysis Date = 08/21/15 
 Pct Recovery = 94%  Analysis Date = 08/17/15 
 Pct Recovery = 94%  Analysis Date = 08/17/15 
 Pct Recovery = 94%  Analysis Date = 08/13/15 
 Pct Recovery = 94%  Analysis Date = 08/13/15 
 Pct Recovery = 94%  Analysis Date = 08/09/15 
 Pct Recovery = 94%  Analysis Date = 08/09/15 
 Pct Recovery = 94%  Analysis Date = 08/05/15 
 Pct Recovery = 95%  Analysis Date = 08/05/15 
 Pct Recovery = 95%  Analysis Date = 08/01/15 
 Pct Recovery = 95%  Analysis Date = 08/01/15 
 Pct Recovery = 95%  Analysis Date = 07/28/15 
 Pct Recovery = 95%  Analysis Date = 07/28/15 
 Pct Recovery = 95%  Analysis Date = 07/23/15 
 Pct Recovery = 95%  Analysis Date = 07/23/15 
 Pct Recovery = 95%  Analysis Date = 07/19/15 
 Pct Recovery = 95%  Analysis Date = 07/19/15 
 Pct Recovery = 95%  Analysis Date = 07/15/15 
 Pct Recovery = 95%  Analysis Date = 07/15/15 
 Pct Recovery = 95%  Analysis Date = 07/11/15 
 Pct Recovery = 95%  Analysis Date = 07/11/15 
 Pct Recovery = 95%  Analysis Date = 07/07/15 
 Pct Recovery = 95%  Analysis Date = 07/07/15 
 Pct Recovery = 95%  Analysis Date = 07/03/15 
 Pct Recovery = 95%  Analysis Date = 07/03/15 
 Pct Recovery = 95%  Analysis Date = 06/29/15 
 Pct Recovery = 96%  Analysis Date = 06/29/15 
 Pct Recovery = 96%  Analysis Date = 06/24/15 
 Pct Recovery = 96%  Analysis Date = 06/24/15 
 Pct Recovery = 96%  Analysis Date = 06/20/15 
 Pct Recovery = 96%  Analysis Date = 06/20/15 
 Pct Recovery = 96%  Analysis Date = 06/16/15 
 Pct Recovery = 96%  Analysis Date = 06/16/15 
 Pct Recovery = 96%  Analysis Date = 06/12/15 
 Pct Recovery = 96%  Analysis Date = 06/12/15 
 Pct Recovery = 96%  Analysis Date = 06/08/15 
 Pct Recovery = 96%  Analysis Date = 06/08/15 
 Pct Recovery = 96%  Analysis Date = 06/04/15 
 Pct Recovery = 96%  Analysis Date = 06/04/15 
 Pct Recovery = 96%  Analysis Date = 05/31/15 
 Pct Recovery = 96%  Analysis Date = 05/31/15 
 Pct Recovery = 96%  Analysis Date = 05/27/15 
 Pct Recovery = 96%  Analysis Date = 05/27/15 
 Pct Recovery = 96%  Analysis Date = 05/22/15 
 Pct Recovery = 97%  Analysis Date = 05/22/15 
 Pct Recovery = 97%  Analysis Date = 05/18/15 
 Pct Recovery = 97%  Analysis Date = 05/18/15 
 Pct Recovery = 97%  Analysis Date = 05/14/15 
 Pct Recovery = 97%  Analysis Date = 05/14/15 
 Pct Recovery = 97%  Analysis Date = 05/10/15 
 Pct Recovery = 97%  Analysis Date = 05/10/15 
 Pct Recovery = 97%  Analysis Date = 05/06/15 
 Pct Recovery = 97%  Analysis Date = 05/06/15 
 Pct Recovery = 97%  Analysis Date = 05/02/15 
 Pct Recovery = 98%  Analysis Date = 05/02/15 
 Pct Recovery = 98%  Analysis Date = 04/28/15 
 Pct Recovery = 98%  Analysis Date = 04/28/15 
 Pct Recovery = 98%  Analysis Date = 04/23/15 
 Pct Recovery = 98%  Analysis Date = 04/23/15 
 Pct Recovery = 98%  Analysis Date = 04/19/15 
 Pct Recovery = 98%  Analysis Date = 04/19/15 
 Pct Recovery = 98%  Analysis Date = 04/15/15 
 Pct Recovery = 98%  Analysis Date = 04/15/15 
 Pct Recovery = 98%  Analysis Date = 04/11/15 
 Pct Recovery = 98%  Analysis Date = 04/11/15 
 Pct Recovery = 98%  Analysis Date = 04/07/15 
 Pct Recovery = 98%  Analysis Date = 04/07/15 
 Pct Recovery = 98%  Analysis Date = 04/03/15 
 Pct Recovery = 98%  Analysis Date = 04/03/15 
 Pct Recovery = 98%  Analysis Date = 03/30/15 
 Pct Recovery = 99%  Analysis Date = 03/30/15 
 Pct Recovery = 99%  Analysis Date = 03/25/15 
 Pct Recovery = 99%  Analysis Date = 03/25/15 
 Pct Recovery = 99%  Analysis Date = 03/21/15 
 Pct Recovery = 99%  Analysis Date = 03/21/15 
 Pct Recovery = 99%  Analysis Date = 03/17/15 
 Pct Recovery = 99%  Analysis Date = 03/17/15 
 Pct Recovery = 99%  Analysis Date = 03/13/15 
 Pct Recovery = 99%  Analysis Date = 03/13/15 
 Pct Recovery = 99%  Analysis Date = 03/09/15 
 Pct Recovery = 99%  Analysis Date = 03/09/15 
 Pct Recovery = 99%  Analysis Date = 03/05/15 
 Pct Recovery = 99%  Analysis Date = 03/05/15 
 Pct Recovery = 99%  Analysis Date = 03/01/15 
 Pct Recovery = 100%  Analysis Date = 03/01/15 
 Pct Recovery = 100%  Analysis Date = 02/24/15 
 Pct Recovery = 100%  Analysis Date = 02/24/15 
 Pct Recovery = 100%  Analysis Date = 02/20/15 
 Pct Recovery = 100%  Analysis Date = 02/20/15 
 Pct Recovery = 100%  Analysis Date = 02/16/15 
 Pct Recovery = 100%  Analysis Date = 02/16/15 
 Pct Recovery = 100%  Analysis Date = 02/12/15 
 Pct Recovery = 100%  Analysis Date = 02/12/15 
 Pct Recovery = 100%  Analysis Date = 02/08/15 
 Pct Recovery = 100%  Analysis Date = 02/08/15 
 Pct Recovery = 100%  Analysis Date = 02/04/15 
 Pct Recovery = 100%  Analysis Date = 02/04/15 
 Pct Recovery = 100%  Analysis Date = 01/31/15 
 Pct Recovery = 101%  Analysis Date = 01/31/15 
 Pct Recovery = 101%  Analysis Date = 01/26/15 
 Pct Recovery = 101%  Analysis Date = 01/26/15 
 Pct Recovery = 101%  Analysis Date = 01/22/15 
 Pct Recovery = 101%  Analysis Date = 01/22/15 
 Pct Recovery = 101%  Analysis Date = 01/18/15 
 Pct Recovery = 101%  Analysis Date = 01/18/15 
 Pct Recovery = 101%  Analysis Date = 01/14/15 
 Pct Recovery = 101%  Analysis Date = 01/14/15 
 Pct Recovery = 101%  Analysis Date = 01/10/15 
 Pct Recovery = 101%  Analysis Date = 01/10/15 
 Pct Recovery = 101%  Analysis Date = 01/06/15 
 Pct Recovery = 101%  Analysis Date = 01/06/15 
 Pct Recovery = 101%  Analysis Date = 01/02/15 
 Pct Recovery = 101%  Analysis Date = 01/02/15 
 Pct Recovery = 101%  Analysis Date = 12/28/14 
 Pct Recovery = 101%  Analysis Date = 12/28/14 
 Pct Recovery = 101%  Analysis Date = 12/24/14 
 Pct Recovery = 101%  Analysis Date = 12/24/14 
 Pct Recovery = 101%  Analysis Date = 12/20/14 
 Pct Recovery = 101%  Analysis Date = 12/20/14 
 Pct Recovery = 101%  Analysis Date = 12/16/14 
 Pct Recovery = 101%  Analysis Date = 12/16/14 
 Pct Recovery = 101%  Analysis Date = 12/12/14 
 Pct Recovery = 101%  Analysis Date = 12/12/14 
 Pct Recovery = 101%  Analysis Date = 12/08/14 
 Pct Recovery = 101%  Analysis Date = 12/08/14 
 Pct Recovery = 101%  Analysis Date = 12/04/14 
 Pct Recovery = 101%  Analysis Date = 12/04/14 
 Pct Recovery = 101%  Analysis Date = 11/29/14 
 Pct Recovery = 101%  Analysis Date = 11/29/14 
 Pct Recovery = 101%  Analysis Date = 11/25/14 
 Pct Recovery = 101%  Analysis Date = 11/25/14 
 Pct Recovery = 101%  Analysis Date = 11/21/14 
 Pct Recovery = 101%  Analysis Date = 11/21/14 
 Pct Recovery = 101%  Analysis Date = 11/17/14 
 Pct Recovery = 101%  Analysis Date = 11/17/14 
 Pct Recovery = 101%  Analysis Date = 11/13/14 
 Pct Recovery = 101%  Analysis Date = 11/13/14 
 Pct Recovery = 101%  Analysis Date = 11/09/14 
 Pct Recovery = 101%  Analysis Date = 11/09/14 
 Pct Recovery = 101%  Analysis Date = 11/05/14 
 Pct Recovery = 101%  Analysis Date = 11/05/14 
 Pct Recovery = 101%  Analysis Date = 11/01/14 
 Pct Recovery = 101%  Analysis Date = 11/01/14 
 Pct Recovery = 101%  Analysis Date = 10/27/14 
 Pct Recovery = 101%  Analysis Date = 10/27/14 
 Pct Recovery = 101%  Analysis Date = 10/23/14 
 Pct Recovery = 101%  Analysis Date = 10/23/14 
 Pct Recovery = 101%  Analysis Date = 10/19/14 
 Pct Recovery = 101%  Analysis Date = 10/19/14 
 Pct Recovery = 101%  Analysis Date = 10/15/14 
 Pct Recovery = 101%  Analysis Date = 10/15/14 
 Pct Recovery = 101%  Analysis Date = 10/11/14 
 Pct Recovery = 101%  Analysis Date = 10/11/14 
 Pct Recovery = 101%  Analysis Date = 10/07/14 
 Pct Recovery = 101%  Analysis Date = 10/07/14 
 Pct Recovery = 101%  Analysis Date = 10/03/14 
 Pct Recovery = 101%  Analysis Date = 10/03/14 
 Pct Recovery = 101%  Analysis Date = 09/28/14 
 Pct Recovery = 101%  Analysis Date = 09/28/14 
 Pct Recovery = 101%  Analysis Date = 09/24/14 
 Pct Recovery = 101%  Analysis Date = 09/24/14 
 Pct Recovery = 101%  Analysis Date = 09/20/14 
 Pct Recovery = 101%  Analysis Date = 09/20/14 
 Pct Recovery = 101%  Analysis Date = 09/16/14 
 Pct Recovery = 101%  Analysis Date = 09/16/14 
 Pct Recovery = 101%  Analysis Date = 09/12/14 
 Pct Recovery = 101%  Analysis Date = 09/12/14 
 Pct Recovery = 101%  Analysis Date = 09/08/14 
 Pct Recovery = 101%  Analysis Date = 09/08/14 
 Pct Recovery = 101%  Analysis Date = 09/04/14 
 Pct Recovery = 101%  Analysis Date = 09/04/14 
 Pct Recovery = 101%  Analysis Date = 08/30/14 
 Pct Recovery = 101%  Analysis Date = 08/30/14 
 Pct Recovery = 101%  Analysis Date = 08/26/14 
 Pct Recovery = 101%  Analysis Date = 08/26/14 
 Pct Recovery = 101%  Analysis Date = 08/22/14 
 Pct Recovery = 101%  Analysis Date = 08/22/14 
 Pct Recovery = 101%  Analysis Date = 08/18/14 
 Pct Recovery = 101%  Analysis Date = 08/18/14 
 Pct Recovery = 101%  Analysis Date = 08/14/14 
 Pct Recovery = 101%  Analysis Date = 08/14/14 
 Pct Recovery = 101%  Analysis Date = 08/10/14 
 Pct Recovery = 101%  Analysis Date = 08/10/14 
 Pct Recovery = 101%  Analysis Date = 08/06/14 
 Pct Recovery = 101%  Analysis Date = 08/06/14 
 Pct Recovery = 101%  Analysis Date = 08/01/14 
 Pct Recovery = 101%  Analysis Date = 08/01/14 
 Pct Recovery = 101%  Analysis Date = 07/28/14 
 Pct Recovery = 101%  Analysis Date = 07/28/14 
 Pct Recovery = 101%  Analysis Date = 07/24/14 
 Pct Recovery = 101%  Analysis Date = 07/24/14 
 Pct Recovery = 101%  Analysis Date = 07/20/14 
 Pct Recovery = 101%  Analysis Date = 07/20/14 
 Pct Recovery = 101%  Analysis Date = 07/16/14 
 Pct Recovery = 101%  Analysis Date = 07/16/14 
 Pct Recovery = 101%  Analysis Date = 07/12/14 
 Pct Recovery = 101%  Analysis Date = 07/12/14 
 Pct Recovery = 101%  Analysis Date = 07/08/14 
 Pct Recovery = 101%  Analysis Date = 07/08/14 
 Pct Recovery = 101%  Analysis Date = 07/03/14 
 Pct Recovery = 101%  Analysis Date = 07/03/14 
 Pct Recovery = 101%  Analysis Date = 06/29/14 
 Pct Recovery = 101%  Analysis Date = 06/29/14 
 Pct Recovery = 101%  Analysis Date = 06/25/14 
 Pct Recovery = 101%  Analysis Date = 06/25/14 
 Pct Recovery = 101%  Analysis Date = 06/21/14 
 Pct Recovery = 101%  Analysis Date = 06/21/14 
 Pct Recovery = 101%  Analysis Date = 06/17/14 
 Pct Recovery = 101%  Analysis Date = 06/17/14 
 Pct Recovery = 101%  Analysis Date = 06/13/14 
 Pct Recovery = 101%  Analysis Date = 06/13/14 
 Pct Recovery = 101%  Analysis Date = 06/09/14 
 Pct Recovery = 101%  Analysis Date = 06/09/14 
 Pct Recovery = 101%  Analysis Date = 06/04/14 
 Pct Recovery = 101%  Analysis Date = 06/04/14 
 Pct Recovery = 101%  Analysis Date = 05/31/14 
 Pct Recovery = 101%  Analysis Date = 05/31/14 
 Pct Recovery = 101%  Analysis Date = 05/27/14 
 Pct Recovery = 101%  Analysis Date = 05/27/14 
 Pct Recovery = 101%  Analysis Date = 05/23/14 
 Pct Recovery = 101%  Analysis Date = 05/23/14 
 Pct Recovery = 101%  Analysis Date = 05/19/14 
 Pct Recovery = 101%  Analysis Date = 05/19/14 
 Pct Recovery = 101%  Analysis Date = 05/15/14 
 Pct Recovery = 101%  Analysis Date = 05/15/14 
 Pct Recovery = 101%  Analysis Date = 05/11/14 
 Pct Recovery = 101%  Analysis Date = 05/11/14 
 Pct Recovery = 101%  Analysis Date = 05/07/14 
 Pct Recovery = 101%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
2-PROPEN-1-OL

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 2 99% 2% 99% 2%
>= Reporting Level 28 94% 11% 93% 8%
Total 30 94% 11% 94% 8%

Sample Statistics
2-PROPEN-1-OL

Characteristic N % % Basis
Plotted 30 86% Spiked
Estimated Values 3 9% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 3 9% Spiked
Spiked 35 .  
False Negatives 2 6% 2 out of 35
Not Spiked 20 .  
False Positives 0 0% 0 out of 20

BQS OBSP Determination:
4-HEPTANONE, 2,6-DIMETHYL-
METHOD: 4437 , TESTIDCODE: 77419GM016
Open Data Set

 Analysis Date = 06/29/16 
 SpikeMix = NSI 041516: 40 µl & ChemService 5082800: 40 µl 
 Pct Recovery = 101%  Analysis Date = 01/10/15 
 SpikeMix = Abs 032014: 20 µl & ERA 0321-14-05A: 20 µl 
 Pct Recovery = 90%  Analysis Date = 08/13/14 
 SpikeMix = ERA 0321-14-05: 20 µl & Accu 214031128: 20 µl 
 Pct Recovery = 99%  Analysis Date = 07/14/16 
 SpikeMix = NSI 041516: 25 µl & ChemService 5082800: 25 µl & NSI 041416HVOC: 25 µl 
 Pct Recovery = 88%  Analysis Date = 08/11/16 
 SpikeMix = Phenova B20160303: 25 µl & Supelco LC20145V: 25 µl & NSI 041416HVOC: 25 µl 
 Pct Recovery = 88%  Analysis Date = 07/11/14 
 SpikeMix = ChemService 2615700: 20 µl & Accu 214031128: 20 µl 
 Pct Recovery = 119%  Analysis Date = 07/03/14 
 SpikeMix = Abs 032014: 20 µl & ChemService 2615700: 20 µl 
 Pct Recovery = 105%  Analysis Date = 06/07/14 
 SpikeMix = ChemService 2615700: 20 µl & Supelco LC06437: 20 µl 
 Pct Recovery = 113%  Analysis Date = 06/06/14 
 SpikeMix = NSI 031814: 20 µl & ChemService 2615700: 20 µl 
 Pct Recovery = 104%  Analysis Date = 10/09/15 
 SpikeMix = Supelco LC13544: 25 µl & NSI 050515HVOC: 25 µl 
 Pct Recovery = 109%  Analysis Date = 10/09/15 
 SpikeMix = ERA 0601-15-05: 25 µl & Accu 215041338: 25 µl 
 Pct Recovery = 87%  Analysis Date = 06/26/15 
 SpikeMix = ChemService 3818700: 25 µl & Accu 215041338: 25 µl 
 Pct Recovery = 90%  Analysis Date = 07/27/16 
 SpikeMix = ChemService 5082800: 15 µl & Supelco LC20145V: 15 µl & Accu 216041225: 15 µl 
 Pct Recovery = 92%  Analysis Date = 06/23/16 
 SpikeMix = . 
 Pct Recovery = 96%  Analysis Date = 07/06/16 
 SpikeMix = Phenova B20160303: 15 µl & Accu 216041354: 15 µl & NSI 041416HVOC: 15 µl 
 Pct Recovery = 89%  Analysis Date = 06/03/16 
 SpikeMix = NSI 041516: 15 µl & Phenova B20160303: 15 µl & NSI 041416HVOC: 15 µl 
 Pct Recovery = 91%  Analysis Date = 04/28/16 
 SpikeMix = ChemService 3818700: 15 µl & Supelco LC13544: 15 µl 
 Pct Recovery = 99%  Analysis Date = 08/24/15 
 SpikeMix = ERA 0601-15-05: 15 µl & Supelco LC13544: 15 µl 
 Pct Recovery = 102%  Analysis Date = 07/30/15 
 SpikeMix = Supelco LC13544: 15 µl & NSI 050515HVOC: 15 µl 
 Pct Recovery = 93%  Analysis Date = 05/14/15 
 SpikeMix = ChemService 3818700: 15 µl & Supelco LC13544: 15 µl 
 Pct Recovery = 111%  Analysis Date = 11/25/15 
 SpikeMix = Accu 215041338: 15 µl & Abs 040315: 15 µl 
 Pct Recovery = 83%  Analysis Date = 09/05/15 
 SpikeMix = Accu 215041338: 15 µl & NSI 050515HVOC: 15 µl 
 Pct Recovery = 83%  Analysis Date = 04/25/15 
 SpikeMix = Abs 032014: 10 µl & ERA 0321-14-05A: 10 µl 
 Pct Recovery = 107%  Analysis Date = 10/21/14 
 SpikeMix = ERA 0321-14-05A: 10 µl & Accu 214031128: 10 µl 
 Pct Recovery = 92%  Analysis Date = 09/06/14 
 SpikeMix = ERA 0321-14-05: 10 µl & Supelco LC06437: 10 µl 
 Pct Recovery = 117%  Analysis Date = 11/22/14 
 SpikeMix = ChemService 2615700: 10 µl & Supelco LC06437: 10 µl 
 Pct Recovery = 97%  Analysis Date = 07/30/14 
 SpikeMix = NSI 031814: 10 µl & ChemService 2615700: 10 µl 
 Pct Recovery = 120%  Analysis Date = 05/20/14 
 SpikeMix = ChemService 2615700: 10 µl & Accu 214031128: 10 µl 
 Pct Recovery = 109%  Analysis Date = 03/22/16 
 SpikeMix = Supelco LC13544: 10 µl & NSI 050515HVOC: 10 µl 
 Pct Recovery = 108%  Analysis Date = 12/10/15 
 SpikeMix = ChemService 3818700: 10 µl & Supelco LC13544: 10 µl 
 Pct Recovery = 111%  Analysis Date = 05/05/15 
 SpikeMix = Supelco LC13544: 10 µl & Abs 040315: 10 µl 
 Pct Recovery = 102%  Analysis Date = 02/12/16 
 SpikeMix = ERA 0601-15-05: 10 µl & Accu 215041338: 10 µl 
 Pct Recovery = 86%  Analysis Date = 01/05/16 
 SpikeMix = Accu 215041338: 10 µl & Abs 040315: 10 µl 
 Pct Recovery = 92%  Analysis Date = 05/20/15 
 SpikeMix = ChemService 3818700: 10 µl & Accu 215041338: 10 µl 
 Pct Recovery = 102%  Analysis Date = 08/10/16 
 Pct Recovery = 93%  Analysis Date = 08/06/16 
 Pct Recovery = 93%  Analysis Date = 08/06/16 
 Pct Recovery = 93%  Analysis Date = 08/02/16 
 Pct Recovery = 93%  Analysis Date = 08/02/16 
 Pct Recovery = 93%  Analysis Date = 07/29/16 
 Pct Recovery = 93%  Analysis Date = 07/29/16 
 Pct Recovery = 93%  Analysis Date = 07/25/16 
 Pct Recovery = 93%  Analysis Date = 07/25/16 
 Pct Recovery = 93%  Analysis Date = 07/21/16 
 Pct Recovery = 93%  Analysis Date = 07/21/16 
 Pct Recovery = 93%  Analysis Date = 07/17/16 
 Pct Recovery = 93%  Analysis Date = 07/17/16 
 Pct Recovery = 93%  Analysis Date = 07/13/16 
 Pct Recovery = 93%  Analysis Date = 07/13/16 
 Pct Recovery = 93%  Analysis Date = 07/09/16 
 Pct Recovery = 93%  Analysis Date = 07/09/16 
 Pct Recovery = 93%  Analysis Date = 07/05/16 
 Pct Recovery = 93%  Analysis Date = 07/05/16 
 Pct Recovery = 93%  Analysis Date = 07/01/16 
 Pct Recovery = 93%  Analysis Date = 07/01/16 
 Pct Recovery = 93%  Analysis Date = 06/27/16 
 Pct Recovery = 93%  Analysis Date = 06/27/16 
 Pct Recovery = 93%  Analysis Date = 06/23/16 
 Pct Recovery = 93%  Analysis Date = 06/23/16 
 Pct Recovery = 93%  Analysis Date = 06/19/16 
 Pct Recovery = 93%  Analysis Date = 06/19/16 
 Pct Recovery = 93%  Analysis Date = 06/15/16 
 Pct Recovery = 93%  Analysis Date = 06/15/16 
 Pct Recovery = 93%  Analysis Date = 06/10/16 
 Pct Recovery = 94%  Analysis Date = 06/10/16 
 Pct Recovery = 94%  Analysis Date = 06/06/16 
 Pct Recovery = 94%  Analysis Date = 06/06/16 
 Pct Recovery = 94%  Analysis Date = 06/02/16 
 Pct Recovery = 94%  Analysis Date = 06/02/16 
 Pct Recovery = 94%  Analysis Date = 05/29/16 
 Pct Recovery = 94%  Analysis Date = 05/29/16 
 Pct Recovery = 94%  Analysis Date = 05/25/16 
 Pct Recovery = 94%  Analysis Date = 05/25/16 
 Pct Recovery = 94%  Analysis Date = 05/21/16 
 Pct Recovery = 94%  Analysis Date = 05/21/16 
 Pct Recovery = 94%  Analysis Date = 05/17/16 
 Pct Recovery = 94%  Analysis Date = 05/17/16 
 Pct Recovery = 94%  Analysis Date = 05/13/16 
 Pct Recovery = 94%  Analysis Date = 05/13/16 
 Pct Recovery = 94%  Analysis Date = 05/09/16 
 Pct Recovery = 94%  Analysis Date = 05/09/16 
 Pct Recovery = 94%  Analysis Date = 05/05/16 
 Pct Recovery = 94%  Analysis Date = 05/05/16 
 Pct Recovery = 94%  Analysis Date = 05/01/16 
 Pct Recovery = 94%  Analysis Date = 05/01/16 
 Pct Recovery = 94%  Analysis Date = 04/27/16 
 Pct Recovery = 94%  Analysis Date = 04/27/16 
 Pct Recovery = 94%  Analysis Date = 04/23/16 
 Pct Recovery = 94%  Analysis Date = 04/23/16 
 Pct Recovery = 94%  Analysis Date = 04/19/16 
 Pct Recovery = 94%  Analysis Date = 04/19/16 
 Pct Recovery = 94%  Analysis Date = 04/14/16 
 Pct Recovery = 94%  Analysis Date = 04/14/16 
 Pct Recovery = 94%  Analysis Date = 04/10/16 
 Pct Recovery = 94%  Analysis Date = 04/10/16 
 Pct Recovery = 94%  Analysis Date = 04/06/16 
 Pct Recovery = 94%  Analysis Date = 04/06/16 
 Pct Recovery = 94%  Analysis Date = 04/02/16 
 Pct Recovery = 94%  Analysis Date = 04/02/16 
 Pct Recovery = 94%  Analysis Date = 03/29/16 
 Pct Recovery = 94%  Analysis Date = 03/29/16 
 Pct Recovery = 94%  Analysis Date = 03/25/16 
 Pct Recovery = 94%  Analysis Date = 03/25/16 
 Pct Recovery = 94%  Analysis Date = 03/21/16 
 Pct Recovery = 94%  Analysis Date = 03/21/16 
 Pct Recovery = 94%  Analysis Date = 03/17/16 
 Pct Recovery = 95%  Analysis Date = 03/17/16 
 Pct Recovery = 95%  Analysis Date = 03/13/16 
 Pct Recovery = 95%  Analysis Date = 03/13/16 
 Pct Recovery = 95%  Analysis Date = 03/09/16 
 Pct Recovery = 95%  Analysis Date = 03/09/16 
 Pct Recovery = 95%  Analysis Date = 03/05/16 
 Pct Recovery = 95%  Analysis Date = 03/05/16 
 Pct Recovery = 95%  Analysis Date = 03/01/16 
 Pct Recovery = 95%  Analysis Date = 03/01/16 
 Pct Recovery = 95%  Analysis Date = 02/26/16 
 Pct Recovery = 95%  Analysis Date = 02/26/16 
 Pct Recovery = 95%  Analysis Date = 02/22/16 
 Pct Recovery = 95%  Analysis Date = 02/22/16 
 Pct Recovery = 95%  Analysis Date = 02/17/16 
 Pct Recovery = 95%  Analysis Date = 02/17/16 
 Pct Recovery = 95%  Analysis Date = 02/13/16 
 Pct Recovery = 95%  Analysis Date = 02/13/16 
 Pct Recovery = 95%  Analysis Date = 02/09/16 
 Pct Recovery = 95%  Analysis Date = 02/09/16 
 Pct Recovery = 95%  Analysis Date = 02/05/16 
 Pct Recovery = 95%  Analysis Date = 02/05/16 
 Pct Recovery = 95%  Analysis Date = 02/01/16 
 Pct Recovery = 95%  Analysis Date = 02/01/16 
 Pct Recovery = 95%  Analysis Date = 01/28/16 
 Pct Recovery = 95%  Analysis Date = 01/28/16 
 Pct Recovery = 95%  Analysis Date = 01/24/16 
 Pct Recovery = 95%  Analysis Date = 01/24/16 
 Pct Recovery = 95%  Analysis Date = 01/20/16 
 Pct Recovery = 95%  Analysis Date = 01/20/16 
 Pct Recovery = 95%  Analysis Date = 01/16/16 
 Pct Recovery = 95%  Analysis Date = 01/16/16 
 Pct Recovery = 95%  Analysis Date = 01/12/16 
 Pct Recovery = 95%  Analysis Date = 01/12/16 
 Pct Recovery = 95%  Analysis Date = 01/08/16 
 Pct Recovery = 95%  Analysis Date = 01/08/16 
 Pct Recovery = 95%  Analysis Date = 01/04/16 
 Pct Recovery = 95%  Analysis Date = 01/04/16 
 Pct Recovery = 95%  Analysis Date = 12/31/15 
 Pct Recovery = 95%  Analysis Date = 12/31/15 
 Pct Recovery = 95%  Analysis Date = 12/27/15 
 Pct Recovery = 95%  Analysis Date = 12/27/15 
 Pct Recovery = 95%  Analysis Date = 12/23/15 
 Pct Recovery = 95%  Analysis Date = 12/23/15 
 Pct Recovery = 95%  Analysis Date = 12/18/15 
 Pct Recovery = 95%  Analysis Date = 12/18/15 
 Pct Recovery = 95%  Analysis Date = 12/14/15 
 Pct Recovery = 95%  Analysis Date = 12/14/15 
 Pct Recovery = 95%  Analysis Date = 12/10/15 
 Pct Recovery = 95%  Analysis Date = 12/10/15 
 Pct Recovery = 95%  Analysis Date = 12/06/15 
 Pct Recovery = 95%  Analysis Date = 12/06/15 
 Pct Recovery = 95%  Analysis Date = 12/02/15 
 Pct Recovery = 95%  Analysis Date = 12/02/15 
 Pct Recovery = 95%  Analysis Date = 11/28/15 
 Pct Recovery = 95%  Analysis Date = 11/28/15 
 Pct Recovery = 95%  Analysis Date = 11/24/15 
 Pct Recovery = 95%  Analysis Date = 11/24/15 
 Pct Recovery = 95%  Analysis Date = 11/20/15 
 Pct Recovery = 95%  Analysis Date = 11/20/15 
 Pct Recovery = 95%  Analysis Date = 11/16/15 
 Pct Recovery = 95%  Analysis Date = 11/16/15 
 Pct Recovery = 95%  Analysis Date = 11/12/15 
 Pct Recovery = 96%  Analysis Date = 11/12/15 
 Pct Recovery = 96%  Analysis Date = 11/08/15 
 Pct Recovery = 96%  Analysis Date = 11/08/15 
 Pct Recovery = 96%  Analysis Date = 11/04/15 
 Pct Recovery = 96%  Analysis Date = 11/04/15 
 Pct Recovery = 96%  Analysis Date = 10/31/15 
 Pct Recovery = 96%  Analysis Date = 10/31/15 
 Pct Recovery = 96%  Analysis Date = 10/27/15 
 Pct Recovery = 96%  Analysis Date = 10/27/15 
 Pct Recovery = 96%  Analysis Date = 10/22/15 
 Pct Recovery = 96%  Analysis Date = 10/22/15 
 Pct Recovery = 96%  Analysis Date = 10/18/15 
 Pct Recovery = 96%  Analysis Date = 10/18/15 
 Pct Recovery = 96%  Analysis Date = 10/14/15 
 Pct Recovery = 96%  Analysis Date = 10/14/15 
 Pct Recovery = 96%  Analysis Date = 10/10/15 
 Pct Recovery = 96%  Analysis Date = 10/10/15 
 Pct Recovery = 96%  Analysis Date = 10/06/15 
 Pct Recovery = 96%  Analysis Date = 10/06/15 
 Pct Recovery = 96%  Analysis Date = 10/02/15 
 Pct Recovery = 96%  Analysis Date = 10/02/15 
 Pct Recovery = 96%  Analysis Date = 09/28/15 
 Pct Recovery = 96%  Analysis Date = 09/28/15 
 Pct Recovery = 96%  Analysis Date = 09/24/15 
 Pct Recovery = 97%  Analysis Date = 09/24/15 
 Pct Recovery = 97%  Analysis Date = 09/20/15 
 Pct Recovery = 97%  Analysis Date = 09/20/15 
 Pct Recovery = 97%  Analysis Date = 09/16/15 
 Pct Recovery = 97%  Analysis Date = 09/16/15 
 Pct Recovery = 97%  Analysis Date = 09/12/15 
 Pct Recovery = 97%  Analysis Date = 09/12/15 
 Pct Recovery = 97%  Analysis Date = 09/08/15 
 Pct Recovery = 97%  Analysis Date = 09/08/15 
 Pct Recovery = 97%  Analysis Date = 09/04/15 
 Pct Recovery = 97%  Analysis Date = 09/04/15 
 Pct Recovery = 97%  Analysis Date = 08/31/15 
 Pct Recovery = 97%  Analysis Date = 08/31/15 
 Pct Recovery = 97%  Analysis Date = 08/26/15 
 Pct Recovery = 97%  Analysis Date = 08/26/15 
 Pct Recovery = 97%  Analysis Date = 08/22/15 
 Pct Recovery = 97%  Analysis Date = 08/22/15 
 Pct Recovery = 97%  Analysis Date = 08/18/15 
 Pct Recovery = 97%  Analysis Date = 08/18/15 
 Pct Recovery = 97%  Analysis Date = 08/14/15 
 Pct Recovery = 97%  Analysis Date = 08/14/15 
 Pct Recovery = 97%  Analysis Date = 08/10/15 
 Pct Recovery = 97%  Analysis Date = 08/10/15 
 Pct Recovery = 97%  Analysis Date = 08/06/15 
 Pct Recovery = 98%  Analysis Date = 08/06/15 
 Pct Recovery = 98%  Analysis Date = 08/02/15 
 Pct Recovery = 98%  Analysis Date = 08/02/15 
 Pct Recovery = 98%  Analysis Date = 07/29/15 
 Pct Recovery = 98%  Analysis Date = 07/29/15 
 Pct Recovery = 98%  Analysis Date = 07/25/15 
 Pct Recovery = 98%  Analysis Date = 07/25/15 
 Pct Recovery = 98%  Analysis Date = 07/21/15 
 Pct Recovery = 98%  Analysis Date = 07/21/15 
 Pct Recovery = 98%  Analysis Date = 07/17/15 
 Pct Recovery = 98%  Analysis Date = 07/17/15 
 Pct Recovery = 98%  Analysis Date = 07/13/15 
 Pct Recovery = 98%  Analysis Date = 07/13/15 
 Pct Recovery = 98%  Analysis Date = 07/09/15 
 Pct Recovery = 98%  Analysis Date = 07/09/15 
 Pct Recovery = 98%  Analysis Date = 07/05/15 
 Pct Recovery = 98%  Analysis Date = 07/05/15 
 Pct Recovery = 98%  Analysis Date = 06/30/15 
 Pct Recovery = 98%  Analysis Date = 06/30/15 
 Pct Recovery = 98%  Analysis Date = 06/26/15 
 Pct Recovery = 98%  Analysis Date = 06/26/15 
 Pct Recovery = 98%  Analysis Date = 06/22/15 
 Pct Recovery = 98%  Analysis Date = 06/22/15 
 Pct Recovery = 98%  Analysis Date = 06/18/15 
 Pct Recovery = 98%  Analysis Date = 06/18/15 
 Pct Recovery = 98%  Analysis Date = 06/14/15 
 Pct Recovery = 98%  Analysis Date = 06/14/15 
 Pct Recovery = 98%  Analysis Date = 06/10/15 
 Pct Recovery = 98%  Analysis Date = 06/10/15 
 Pct Recovery = 98%  Analysis Date = 06/06/15 
 Pct Recovery = 98%  Analysis Date = 06/06/15 
 Pct Recovery = 98%  Analysis Date = 06/02/15 
 Pct Recovery = 98%  Analysis Date = 06/02/15 
 Pct Recovery = 98%  Analysis Date = 05/29/15 
 Pct Recovery = 98%  Analysis Date = 05/29/15 
 Pct Recovery = 98%  Analysis Date = 05/25/15 
 Pct Recovery = 98%  Analysis Date = 05/25/15 
 Pct Recovery = 98%  Analysis Date = 05/21/15 
 Pct Recovery = 98%  Analysis Date = 05/21/15 
 Pct Recovery = 98%  Analysis Date = 05/17/15 
 Pct Recovery = 98%  Analysis Date = 05/17/15 
 Pct Recovery = 98%  Analysis Date = 05/13/15 
 Pct Recovery = 98%  Analysis Date = 05/13/15 
 Pct Recovery = 98%  Analysis Date = 05/09/15 
 Pct Recovery = 98%  Analysis Date = 05/09/15 
 Pct Recovery = 98%  Analysis Date = 05/05/15 
 Pct Recovery = 98%  Analysis Date = 05/05/15 
 Pct Recovery = 98%  Analysis Date = 04/30/15 
 Pct Recovery = 99%  Analysis Date = 04/30/15 
 Pct Recovery = 99%  Analysis Date = 04/26/15 
 Pct Recovery = 99%  Analysis Date = 04/26/15 
 Pct Recovery = 99%  Analysis Date = 04/22/15 
 Pct Recovery = 99%  Analysis Date = 04/22/15 
 Pct Recovery = 99%  Analysis Date = 04/18/15 
 Pct Recovery = 99%  Analysis Date = 04/18/15 
 Pct Recovery = 99%  Analysis Date = 04/14/15 
 Pct Recovery = 99%  Analysis Date = 04/14/15 
 Pct Recovery = 99%  Analysis Date = 04/10/15 
 Pct Recovery = 99%  Analysis Date = 04/10/15 
 Pct Recovery = 99%  Analysis Date = 04/06/15 
 Pct Recovery = 99%  Analysis Date = 04/06/15 
 Pct Recovery = 99%  Analysis Date = 04/02/15 
 Pct Recovery = 100%  Analysis Date = 04/02/15 
 Pct Recovery = 100%  Analysis Date = 03/29/15 
 Pct Recovery = 100%  Analysis Date = 03/29/15 
 Pct Recovery = 100%  Analysis Date = 03/25/15 
 Pct Recovery = 100%  Analysis Date = 03/25/15 
 Pct Recovery = 100%  Analysis Date = 03/21/15 
 Pct Recovery = 100%  Analysis Date = 03/21/15 
 Pct Recovery = 100%  Analysis Date = 03/17/15 
 Pct Recovery = 100%  Analysis Date = 03/17/15 
 Pct Recovery = 100%  Analysis Date = 03/13/15 
 Pct Recovery = 100%  Analysis Date = 03/13/15 
 Pct Recovery = 100%  Analysis Date = 03/09/15 
 Pct Recovery = 100%  Analysis Date = 03/09/15 
 Pct Recovery = 100%  Analysis Date = 03/04/15 
 Pct Recovery = 101%  Analysis Date = 03/04/15 
 Pct Recovery = 101%  Analysis Date = 02/28/15 
 Pct Recovery = 101%  Analysis Date = 02/28/15 
 Pct Recovery = 101%  Analysis Date = 02/24/15 
 Pct Recovery = 101%  Analysis Date = 02/24/15 
 Pct Recovery = 101%  Analysis Date = 02/20/15 
 Pct Recovery = 101%  Analysis Date = 02/20/15 
 Pct Recovery = 101%  Analysis Date = 02/16/15 
 Pct Recovery = 101%  Analysis Date = 02/16/15 
 Pct Recovery = 101%  Analysis Date = 02/12/15 
 Pct Recovery = 101%  Analysis Date = 02/12/15 
 Pct Recovery = 101%  Analysis Date = 02/08/15 
 Pct Recovery = 101%  Analysis Date = 02/08/15 
 Pct Recovery = 101%  Analysis Date = 02/04/15 
 Pct Recovery = 101%  Analysis Date = 02/04/15 
 Pct Recovery = 101%  Analysis Date = 01/31/15 
 Pct Recovery = 102%  Analysis Date = 01/31/15 
 Pct Recovery = 102%  Analysis Date = 01/27/15 
 Pct Recovery = 102%  Analysis Date = 01/27/15 
 Pct Recovery = 102%  Analysis Date = 01/23/15 
 Pct Recovery = 102%  Analysis Date = 01/23/15 
 Pct Recovery = 102%  Analysis Date = 01/19/15 
 Pct Recovery = 102%  Analysis Date = 01/19/15 
 Pct Recovery = 102%  Analysis Date = 01/15/15 
 Pct Recovery = 102%  Analysis Date = 01/15/15 
 Pct Recovery = 102%  Analysis Date = 01/11/15 
 Pct Recovery = 102%  Analysis Date = 01/11/15 
 Pct Recovery = 102%  Analysis Date = 01/06/15 
 Pct Recovery = 102%  Analysis Date = 01/06/15 
 Pct Recovery = 102%  Analysis Date = 01/02/15 
 Pct Recovery = 103%  Analysis Date = 01/02/15 
 Pct Recovery = 103%  Analysis Date = 12/29/14 
 Pct Recovery = 103%  Analysis Date = 12/29/14 
 Pct Recovery = 103%  Analysis Date = 12/25/14 
 Pct Recovery = 103%  Analysis Date = 12/25/14 
 Pct Recovery = 103%  Analysis Date = 12/21/14 
 Pct Recovery = 103%  Analysis Date = 12/21/14 
 Pct Recovery = 103%  Analysis Date = 12/17/14 
 Pct Recovery = 103%  Analysis Date = 12/17/14 
 Pct Recovery = 103%  Analysis Date = 12/13/14 
 Pct Recovery = 103%  Analysis Date = 12/13/14 
 Pct Recovery = 103%  Analysis Date = 12/09/14 
 Pct Recovery = 103%  Analysis Date = 12/09/14 
 Pct Recovery = 103%  Analysis Date = 12/05/14 
 Pct Recovery = 104%  Analysis Date = 12/05/14 
 Pct Recovery = 104%  Analysis Date = 12/01/14 
 Pct Recovery = 104%  Analysis Date = 12/01/14 
 Pct Recovery = 104%  Analysis Date = 11/27/14 
 Pct Recovery = 104%  Analysis Date = 11/27/14 
 Pct Recovery = 104%  Analysis Date = 11/23/14 
 Pct Recovery = 104%  Analysis Date = 11/23/14 
 Pct Recovery = 104%  Analysis Date = 11/19/14 
 Pct Recovery = 104%  Analysis Date = 11/19/14 
 Pct Recovery = 104%  Analysis Date = 11/15/14 
 Pct Recovery = 104%  Analysis Date = 11/15/14 
 Pct Recovery = 104%  Analysis Date = 11/11/14 
 Pct Recovery = 104%  Analysis Date = 11/11/14 
 Pct Recovery = 104%  Analysis Date = 11/06/14 
 Pct Recovery = 104%  Analysis Date = 11/06/14 
 Pct Recovery = 104%  Analysis Date = 11/02/14 
 Pct Recovery = 105%  Analysis Date = 11/02/14 
 Pct Recovery = 105%  Analysis Date = 10/29/14 
 Pct Recovery = 105%  Analysis Date = 10/29/14 
 Pct Recovery = 105%  Analysis Date = 10/25/14 
 Pct Recovery = 105%  Analysis Date = 10/25/14 
 Pct Recovery = 105%  Analysis Date = 10/21/14 
 Pct Recovery = 105%  Analysis Date = 10/21/14 
 Pct Recovery = 105%  Analysis Date = 10/17/14 
 Pct Recovery = 105%  Analysis Date = 10/17/14 
 Pct Recovery = 105%  Analysis Date = 10/13/14 
 Pct Recovery = 105%  Analysis Date = 10/13/14 
 Pct Recovery = 105%  Analysis Date = 10/09/14 
 Pct Recovery = 105%  Analysis Date = 10/09/14 
 Pct Recovery = 105%  Analysis Date = 10/05/14 
 Pct Recovery = 106%  Analysis Date = 10/05/14 
 Pct Recovery = 106%  Analysis Date = 10/01/14 
 Pct Recovery = 106%  Analysis Date = 10/01/14 
 Pct Recovery = 106%  Analysis Date = 09/27/14 
 Pct Recovery = 106%  Analysis Date = 09/27/14 
 Pct Recovery = 106%  Analysis Date = 09/23/14 
 Pct Recovery = 106%  Analysis Date = 09/23/14 
 Pct Recovery = 106%  Analysis Date = 09/19/14 
 Pct Recovery = 106%  Analysis Date = 09/19/14 
 Pct Recovery = 106%  Analysis Date = 09/15/14 
 Pct Recovery = 106%  Analysis Date = 09/15/14 
 Pct Recovery = 106%  Analysis Date = 09/10/14 
 Pct Recovery = 106%  Analysis Date = 09/10/14 
 Pct Recovery = 106%  Analysis Date = 09/06/14 
 Pct Recovery = 107%  Analysis Date = 09/06/14 
 Pct Recovery = 107%  Analysis Date = 09/02/14 
 Pct Recovery = 107%  Analysis Date = 09/02/14 
 Pct Recovery = 107%  Analysis Date = 08/29/14 
 Pct Recovery = 107%  Analysis Date = 08/29/14 
 Pct Recovery = 107%  Analysis Date = 08/25/14 
 Pct Recovery = 107%  Analysis Date = 08/25/14 
 Pct Recovery = 107%  Analysis Date = 08/21/14 
 Pct Recovery = 107%  Analysis Date = 08/21/14 
 Pct Recovery = 107%  Analysis Date = 08/17/14 
 Pct Recovery = 107%  Analysis Date = 08/17/14 
 Pct Recovery = 107%  Analysis Date = 08/13/14 
 Pct Recovery = 107%  Analysis Date = 08/13/14 
 Pct Recovery = 107%  Analysis Date = 08/09/14 
 Pct Recovery = 108%  Analysis Date = 08/09/14 
 Pct Recovery = 108%  Analysis Date = 08/05/14 
 Pct Recovery = 108%  Analysis Date = 08/05/14 
 Pct Recovery = 108%  Analysis Date = 08/01/14 
 Pct Recovery = 108%  Analysis Date = 08/01/14 
 Pct Recovery = 108%  Analysis Date = 07/28/14 
 Pct Recovery = 108%  Analysis Date = 07/28/14 
 Pct Recovery = 108%  Analysis Date = 07/24/14 
 Pct Recovery = 108%  Analysis Date = 07/24/14 
 Pct Recovery = 108%  Analysis Date = 07/20/14 
 Pct Recovery = 108%  Analysis Date = 07/20/14 
 Pct Recovery = 108%  Analysis Date = 07/15/14 
 Pct Recovery = 108%  Analysis Date = 07/15/14 
 Pct Recovery = 108%  Analysis Date = 07/11/14 
 Pct Recovery = 108%  Analysis Date = 07/11/14 
 Pct Recovery = 108%  Analysis Date = 07/07/14 
 Pct Recovery = 109%  Analysis Date = 07/07/14 
 Pct Recovery = 109%  Analysis Date = 07/03/14 
 Pct Recovery = 109%  Analysis Date = 07/03/14 
 Pct Recovery = 109%  Analysis Date = 06/29/14 
 Pct Recovery = 109%  Analysis Date = 06/29/14 
 Pct Recovery = 109%  Analysis Date = 06/25/14 
 Pct Recovery = 109%  Analysis Date = 06/25/14 
 Pct Recovery = 109%  Analysis Date = 06/21/14 
 Pct Recovery = 109%  Analysis Date = 06/21/14 
 Pct Recovery = 109%  Analysis Date = 06/17/14 
 Pct Recovery = 109%  Analysis Date = 06/17/14 
 Pct Recovery = 109%  Analysis Date = 06/13/14 
 Pct Recovery = 110%  Analysis Date = 06/13/14 
 Pct Recovery = 110%  Analysis Date = 06/09/14 
 Pct Recovery = 110%  Analysis Date = 06/09/14 
 Pct Recovery = 110%  Analysis Date = 06/05/14 
 Pct Recovery = 110%  Analysis Date = 06/05/14 
 Pct Recovery = 110%  Analysis Date = 06/01/14 
 Pct Recovery = 110%  Analysis Date = 06/01/14 
 Pct Recovery = 110%  Analysis Date = 05/28/14 
 Pct Recovery = 110%  Analysis Date = 05/28/14 
 Pct Recovery = 110%  Analysis Date = 05/24/14 
 Pct Recovery = 110%  Analysis Date = 05/24/14 
 Pct Recovery = 110%  Analysis Date = 05/20/14 
 Pct Recovery = 111%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
4-HEPTANONE, 2,6-DIMETHYL-

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 34 99% 11% 99% 13%
Total 34 99% 11% 99% 13%

Sample Statistics
4-HEPTANONE, 2,6-DIMETHYL-

Characteristic N % % Basis
Plotted 34 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 34 .  
False Negatives 0 0% 0 out of 34
Not Spiked 21 .  
False Positives 2 10% 2 out of 21

BQS OBSP Determination:
ACETATE, ETHYL
METHOD: 4437 , TESTIDCODE: 81585GM016
Open Data Set

 Analysis Date = 07/14/16 
 SpikeMix = NSI 041516: 25 µl & ChemService 5082800: 25 µl & NSI 041416HVOC: 25 µl 
 Pct Recovery = 640%  Analysis Date = 08/13/14 
 SpikeMix = ERA 0321-14-05: 20 µl & Accu 214031128: 20 µl 
 Pct Recovery = 268%  Analysis Date = 06/07/14 
 SpikeMix = ChemService 2615700: 20 µl & Supelco LC06437: 20 µl 
 Pct Recovery = 546%  Analysis Date = 07/27/16 
 SpikeMix = ChemService 5082800: 15 µl & Supelco LC20145V: 15 µl & Accu 216041225: 15 µl 
 Pct Recovery = 290%  Analysis Date = 10/21/14 
 SpikeMix = ERA 0321-14-05A: 10 µl & Accu 214031128: 10 µl 
 Pct Recovery = 343%  Analysis Date = 09/06/14 
 SpikeMix = ERA 0321-14-05: 10 µl & Supelco LC06437: 10 µl 
 Pct Recovery = 660%  Analysis Date = 11/22/14 
 SpikeMix = ChemService 2615700: 10 µl & Supelco LC06437: 10 µl 
 Pct Recovery = 815%  Analysis Date = 07/29/16 
 SpikeMix = Supelco LC20145V: 40 µl & NSI 041516: 40 µl & NSI 041416HVOC: 40 µl 
 Pct Recovery = 91%  Analysis Date = 07/06/16 
 SpikeMix = Accu 216041354: 40 µl & NSI 041516: 40 µl & NSI 041416HVOC: 40 µl 
 Pct Recovery = 106%  Analysis Date = 08/11/16 
 SpikeMix = Phenova B20160303: 25 µl & Supelco LC20145V: 25 µl & NSI 041416HVOC: 25 µl 
 Pct Recovery = 76%  Analysis Date = 05/21/16 
 SpikeMix = Supelco LC20145V: 25 µl & NSI 041516: 25 µl & NSI 041416HVOC: 25 µl 
 Pct Recovery = 127%  Analysis Date = 01/10/15 
 SpikeMix = Abs 032014: 20 µl & ERA 0321-14-05A: 20 µl 
 Pct Recovery = 136%  Analysis Date = 07/11/14 
 SpikeMix = ChemService 2615700: 20 µl & Accu 214031128: 20 µl 
 Pct Recovery = 131%  Analysis Date = 07/03/14 
 SpikeMix = Abs 032014: 20 µl & ChemService 2615700: 20 µl 
 Pct Recovery = 29%  Analysis Date = 06/06/14 
 SpikeMix = NSI 031814: 20 µl & ChemService 2615700: 20 µl 
 Pct Recovery = 25%  Analysis Date = 10/09/15 
 SpikeMix = Supelco LC13544: 25 µl & NSI 050515HVOC: 25 µl 
 Pct Recovery = 98%  Analysis Date = 10/09/15 
 SpikeMix = ERA 0601-15-05: 25 µl & Accu 215041338: 25 µl 
 Pct Recovery = 80%  Analysis Date = 06/26/15 
 SpikeMix = ChemService 3818700: 25 µl & Accu 215041338: 25 µl 
 Pct Recovery = 97%  Analysis Date = 05/20/16 
 SpikeMix = Accu 216041354: 15 µl & NSI 041516: 15 µl & Accu 216041225: 15 µl 
 Pct Recovery = 144%  Analysis Date = 07/06/16 
 SpikeMix = Phenova B20160303: 15 µl & Accu 216041354: 15 µl & NSI 041416HVOC: 15 µl 
 Pct Recovery = 103%  Analysis Date = 06/03/16 
 SpikeMix = NSI 041516: 15 µl & Phenova B20160303: 15 µl & NSI 041416HVOC: 15 µl 
 Pct Recovery = 111%  Analysis Date = 04/28/16 
 SpikeMix = ChemService 3818700: 15 µl & Supelco LC13544: 15 µl 
 Pct Recovery = 106%  Analysis Date = 08/24/15 
 SpikeMix = ERA 0601-15-05: 15 µl & Supelco LC13544: 15 µl 
 Pct Recovery = 79%  Analysis Date = 07/30/15 
 SpikeMix = Supelco LC13544: 15 µl & NSI 050515HVOC: 15 µl 
 Pct Recovery = 84%  Analysis Date = 05/14/15 
 SpikeMix = ChemService 3818700: 15 µl & Supelco LC13544: 15 µl 
 Pct Recovery = 116%  Analysis Date = 11/25/15 
 SpikeMix = Accu 215041338: 15 µl & Abs 040315: 15 µl 
 Pct Recovery = 101%  Analysis Date = 09/05/15 
 SpikeMix = Accu 215041338: 15 µl & NSI 050515HVOC: 15 µl 
 Pct Recovery = 93%  Analysis Date = 04/25/15 
 SpikeMix = Abs 032014: 10 µl & ERA 0321-14-05A: 10 µl 
 Pct Recovery = 83%  Analysis Date = 05/20/14 
 SpikeMix = ChemService 2615700: 10 µl & Accu 214031128: 10 µl 
 Pct Recovery = 151%  Analysis Date = 03/22/16 
 SpikeMix = Supelco LC13544: 10 µl & NSI 050515HVOC: 10 µl 
 Pct Recovery = 117%  Analysis Date = 12/10/15 
 SpikeMix = ChemService 3818700: 10 µl & Supelco LC13544: 10 µl 
 Pct Recovery = 111%  Analysis Date = 05/05/15 
 SpikeMix = Supelco LC13544: 10 µl & Abs 040315: 10 µl 
 Pct Recovery = 104%  Analysis Date = 02/12/16 
 SpikeMix = ERA 0601-15-05: 10 µl & Accu 215041338: 10 µl 
 Pct Recovery = 86%  Analysis Date = 01/05/16 
 SpikeMix = Accu 215041338: 10 µl & Abs 040315: 10 µl 
 Pct Recovery = 96%  Analysis Date = 05/20/15 
 SpikeMix = ChemService 3818700: 10 µl & Accu 215041338: 10 µl 
 Pct Recovery = 72%  Analysis Date = 08/10/16 
 Pct Recovery = 203%  Analysis Date = 08/06/16 
 Pct Recovery = 201%  Analysis Date = 08/06/16 
 Pct Recovery = 201%  Analysis Date = 08/02/16 
 Pct Recovery = 199%  Analysis Date = 08/02/16 
 Pct Recovery = 199%  Analysis Date = 07/29/16 
 Pct Recovery = 197%  Analysis Date = 07/29/16 
 Pct Recovery = 197%  Analysis Date = 07/25/16 
 Pct Recovery = 195%  Analysis Date = 07/25/16 
 Pct Recovery = 195%  Analysis Date = 07/21/16 
 Pct Recovery = 193%  Analysis Date = 07/21/16 
 Pct Recovery = 193%  Analysis Date = 07/17/16 
 Pct Recovery = 191%  Analysis Date = 07/17/16 
 Pct Recovery = 191%  Analysis Date = 07/13/16 
 Pct Recovery = 189%  Analysis Date = 07/13/16 
 Pct Recovery = 189%  Analysis Date = 07/09/16 
 Pct Recovery = 187%  Analysis Date = 07/09/16 
 Pct Recovery = 187%  Analysis Date = 07/05/16 
 Pct Recovery = 185%  Analysis Date = 07/05/16 
 Pct Recovery = 185%  Analysis Date = 07/01/16 
 Pct Recovery = 183%  Analysis Date = 07/01/16 
 Pct Recovery = 183%  Analysis Date = 06/27/16 
 Pct Recovery = 181%  Analysis Date = 06/27/16 
 Pct Recovery = 181%  Analysis Date = 06/23/16 
 Pct Recovery = 179%  Analysis Date = 06/23/16 
 Pct Recovery = 179%  Analysis Date = 06/19/16 
 Pct Recovery = 177%  Analysis Date = 06/19/16 
 Pct Recovery = 177%  Analysis Date = 06/15/16 
 Pct Recovery = 175%  Analysis Date = 06/15/16 
 Pct Recovery = 175%  Analysis Date = 06/10/16 
 Pct Recovery = 173%  Analysis Date = 06/10/16 
 Pct Recovery = 173%  Analysis Date = 06/06/16 
 Pct Recovery = 171%  Analysis Date = 06/06/16 
 Pct Recovery = 171%  Analysis Date = 06/02/16 
 Pct Recovery = 170%  Analysis Date = 06/02/16 
 Pct Recovery = 170%  Analysis Date = 05/29/16 
 Pct Recovery = 168%  Analysis Date = 05/29/16 
 Pct Recovery = 168%  Analysis Date = 05/25/16 
 Pct Recovery = 166%  Analysis Date = 05/25/16 
 Pct Recovery = 166%  Analysis Date = 05/21/16 
 Pct Recovery = 164%  Analysis Date = 05/21/16 
 Pct Recovery = 164%  Analysis Date = 05/17/16 
 Pct Recovery = 162%  Analysis Date = 05/17/16 
 Pct Recovery = 162%  Analysis Date = 05/13/16 
 Pct Recovery = 160%  Analysis Date = 05/13/16 
 Pct Recovery = 160%  Analysis Date = 05/09/16 
 Pct Recovery = 158%  Analysis Date = 05/09/16 
 Pct Recovery = 158%  Analysis Date = 05/05/16 
 Pct Recovery = 157%  Analysis Date = 05/05/16 
 Pct Recovery = 157%  Analysis Date = 05/01/16 
 Pct Recovery = 155%  Analysis Date = 05/01/16 
 Pct Recovery = 155%  Analysis Date = 04/27/16 
 Pct Recovery = 153%  Analysis Date = 04/27/16 
 Pct Recovery = 153%  Analysis Date = 04/23/16 
 Pct Recovery = 151%  Analysis Date = 04/23/16 
 Pct Recovery = 151%  Analysis Date = 04/19/16 
 Pct Recovery = 150%  Analysis Date = 04/19/16 
 Pct Recovery = 150%  Analysis Date = 04/14/16 
 Pct Recovery = 148%  Analysis Date = 04/14/16 
 Pct Recovery = 148%  Analysis Date = 04/10/16 
 Pct Recovery = 146%  Analysis Date = 04/10/16 
 Pct Recovery = 146%  Analysis Date = 04/06/16 
 Pct Recovery = 144%  Analysis Date = 04/06/16 
 Pct Recovery = 144%  Analysis Date = 04/02/16 
 Pct Recovery = 142%  Analysis Date = 04/02/16 
 Pct Recovery = 142%  Analysis Date = 03/29/16 
 Pct Recovery = 141%  Analysis Date = 03/29/16 
 Pct Recovery = 141%  Analysis Date = 03/25/16 
 Pct Recovery = 139%  Analysis Date = 03/25/16 
 Pct Recovery = 139%  Analysis Date = 03/21/16 
 Pct Recovery = 137%  Analysis Date = 03/21/16 
 Pct Recovery = 137%  Analysis Date = 03/17/16 
 Pct Recovery = 135%  Analysis Date = 03/17/16 
 Pct Recovery = 135%  Analysis Date = 03/13/16 
 Pct Recovery = 133%  Analysis Date = 03/13/16 
 Pct Recovery = 133%  Analysis Date = 03/09/16 
 Pct Recovery = 132%  Analysis Date = 03/09/16 
 Pct Recovery = 132%  Analysis Date = 03/05/16 
 Pct Recovery = 130%  Analysis Date = 03/05/16 
 Pct Recovery = 130%  Analysis Date = 03/01/16 
 Pct Recovery = 128%  Analysis Date = 03/01/16 
 Pct Recovery = 128%  Analysis Date = 02/26/16 
 Pct Recovery = 126%  Analysis Date = 02/26/16 
 Pct Recovery = 126%  Analysis Date = 02/22/16 
 Pct Recovery = 125%  Analysis Date = 02/22/16 
 Pct Recovery = 125%  Analysis Date = 02/17/16 
 Pct Recovery = 123%  Analysis Date = 02/17/16 
 Pct Recovery = 123%  Analysis Date = 02/13/16 
 Pct Recovery = 121%  Analysis Date = 02/13/16 
 Pct Recovery = 121%  Analysis Date = 02/09/16 
 Pct Recovery = 119%  Analysis Date = 02/09/16 
 Pct Recovery = 119%  Analysis Date = 02/05/16 
 Pct Recovery = 117%  Analysis Date = 02/05/16 
 Pct Recovery = 117%  Analysis Date = 02/01/16 
 Pct Recovery = 116%  Analysis Date = 02/01/16 
 Pct Recovery = 116%  Analysis Date = 01/28/16 
 Pct Recovery = 114%  Analysis Date = 01/28/16 
 Pct Recovery = 114%  Analysis Date = 01/24/16 
 Pct Recovery = 112%  Analysis Date = 01/24/16 
 Pct Recovery = 112%  Analysis Date = 01/20/16 
 Pct Recovery = 110%  Analysis Date = 01/20/16 
 Pct Recovery = 110%  Analysis Date = 01/16/16 
 Pct Recovery = 108%  Analysis Date = 01/16/16 
 Pct Recovery = 108%  Analysis Date = 01/12/16 
 Pct Recovery = 107%  Analysis Date = 01/12/16 
 Pct Recovery = 107%  Analysis Date = 01/08/16 
 Pct Recovery = 105%  Analysis Date = 01/08/16 
 Pct Recovery = 105%  Analysis Date = 01/04/16 
 Pct Recovery = 103%  Analysis Date = 01/04/16 
 Pct Recovery = 103%  Analysis Date = 12/31/15 
 Pct Recovery = 103%  Analysis Date = 12/31/15 
 Pct Recovery = 103%  Analysis Date = 12/27/15 
 Pct Recovery = 102%  Analysis Date = 12/27/15 
 Pct Recovery = 102%  Analysis Date = 12/23/15 
 Pct Recovery = 101%  Analysis Date = 12/23/15 
 Pct Recovery = 101%  Analysis Date = 12/18/15 
 Pct Recovery = 101%  Analysis Date = 12/18/15 
 Pct Recovery = 101%  Analysis Date = 12/14/15 
 Pct Recovery = 100%  Analysis Date = 12/14/15 
 Pct Recovery = 100%  Analysis Date = 12/10/15 
 Pct Recovery = 99%  Analysis Date = 12/10/15 
 Pct Recovery = 99%  Analysis Date = 12/06/15 
 Pct Recovery = 99%  Analysis Date = 12/06/15 
 Pct Recovery = 99%  Analysis Date = 12/02/15 
 Pct Recovery = 98%  Analysis Date = 12/02/15 
 Pct Recovery = 98%  Analysis Date = 11/28/15 
 Pct Recovery = 97%  Analysis Date = 11/28/15 
 Pct Recovery = 97%  Analysis Date = 11/24/15 
 Pct Recovery = 97%  Analysis Date = 11/24/15 
 Pct Recovery = 97%  Analysis Date = 11/20/15 
 Pct Recovery = 97%  Analysis Date = 11/20/15 
 Pct Recovery = 97%  Analysis Date = 11/16/15 
 Pct Recovery = 96%  Analysis Date = 11/16/15 
 Pct Recovery = 96%  Analysis Date = 11/12/15 
 Pct Recovery = 96%  Analysis Date = 11/12/15 
 Pct Recovery = 96%  Analysis Date = 11/08/15 
 Pct Recovery = 96%  Analysis Date = 11/08/15 
 Pct Recovery = 96%  Analysis Date = 11/04/15 
 Pct Recovery = 96%  Analysis Date = 11/04/15 
 Pct Recovery = 96%  Analysis Date = 10/31/15 
 Pct Recovery = 96%  Analysis Date = 10/31/15 
 Pct Recovery = 96%  Analysis Date = 10/27/15 
 Pct Recovery = 96%  Analysis Date = 10/27/15 
 Pct Recovery = 96%  Analysis Date = 10/22/15 
 Pct Recovery = 96%  Analysis Date = 10/22/15 
 Pct Recovery = 96%  Analysis Date = 10/18/15 
 Pct Recovery = 95%  Analysis Date = 10/18/15 
 Pct Recovery = 95%  Analysis Date = 10/14/15 
 Pct Recovery = 95%  Analysis Date = 10/14/15 
 Pct Recovery = 95%  Analysis Date = 10/10/15 
 Pct Recovery = 95%  Analysis Date = 10/10/15 
 Pct Recovery = 95%  Analysis Date = 10/06/15 
 Pct Recovery = 95%  Analysis Date = 10/06/15 
 Pct Recovery = 95%  Analysis Date = 10/02/15 
 Pct Recovery = 95%  Analysis Date = 10/02/15 
 Pct Recovery = 95%  Analysis Date = 09/28/15 
 Pct Recovery = 95%  Analysis Date = 09/28/15 
 Pct Recovery = 95%  Analysis Date = 09/24/15 
 Pct Recovery = 95%  Analysis Date = 09/24/15 
 Pct Recovery = 95%  Analysis Date = 09/20/15 
 Pct Recovery = 94%  Analysis Date = 09/20/15 
 Pct Recovery = 94%  Analysis Date = 09/16/15 
 Pct Recovery = 94%  Analysis Date = 09/16/15 
 Pct Recovery = 94%  Analysis Date = 09/12/15 
 Pct Recovery = 94%  Analysis Date = 09/12/15 
 Pct Recovery = 94%  Analysis Date = 09/08/15 
 Pct Recovery = 94%  Analysis Date = 09/08/15 
 Pct Recovery = 94%  Analysis Date = 09/04/15 
 Pct Recovery = 94%  Analysis Date = 09/04/15 
 Pct Recovery = 94%  Analysis Date = 08/31/15 
 Pct Recovery = 97%  Analysis Date = 08/31/15 
 Pct Recovery = 97%  Analysis Date = 08/26/15 
 Pct Recovery = 100%  Analysis Date = 08/26/15 
 Pct Recovery = 100%  Analysis Date = 08/22/15 
 Pct Recovery = 103%  Analysis Date = 08/22/15 
 Pct Recovery = 103%  Analysis Date = 08/18/15 
 Pct Recovery = 105%  Analysis Date = 08/18/15 
 Pct Recovery = 105%  Analysis Date = 08/14/15 
 Pct Recovery = 108%  Analysis Date = 08/14/15 
 Pct Recovery = 108%  Analysis Date = 08/10/15 
 Pct Recovery = 111%  Analysis Date = 08/10/15 
 Pct Recovery = 111%  Analysis Date = 08/06/15 
 Pct Recovery = 113%  Analysis Date = 08/06/15 
 Pct Recovery = 113%  Analysis Date = 08/02/15 
 Pct Recovery = 116%  Analysis Date = 08/02/15 
 Pct Recovery = 116%  Analysis Date = 07/29/15 
 Pct Recovery = 119%  Analysis Date = 07/29/15 
 Pct Recovery = 119%  Analysis Date = 07/25/15 
 Pct Recovery = 121%  Analysis Date = 07/25/15 
 Pct Recovery = 121%  Analysis Date = 07/21/15 
 Pct Recovery = 124%  Analysis Date = 07/21/15 
 Pct Recovery = 124%  Analysis Date = 07/17/15 
 Pct Recovery = 127%  Analysis Date = 07/17/15 
 Pct Recovery = 127%  Analysis Date = 07/13/15 
 Pct Recovery = 130%  Analysis Date = 07/13/15 
 Pct Recovery = 130%  Analysis Date = 07/09/15 
 Pct Recovery = 132%  Analysis Date = 07/09/15 
 Pct Recovery = 132%  Analysis Date = 07/05/15 
 Pct Recovery = 135%  Analysis Date = 07/05/15 
 Pct Recovery = 135%  Analysis Date = 06/30/15 
 Pct Recovery = 138%  Analysis Date = 06/30/15 
 Pct Recovery = 138%  Analysis Date = 06/26/15 
 Pct Recovery = 140%  Analysis Date = 06/26/15 
 Pct Recovery = 140%  Analysis Date = 06/22/15 
 Pct Recovery = 143%  Analysis Date = 06/22/15 
 Pct Recovery = 143%  Analysis Date = 06/18/15 
 Pct Recovery = 146%  Analysis Date = 06/18/15 
 Pct Recovery = 146%  Analysis Date = 06/14/15 
 Pct Recovery = 148%  Analysis Date = 06/14/15 
 Pct Recovery = 148%  Analysis Date = 06/10/15 
 Pct Recovery = 151%  Analysis Date = 06/10/15 
 Pct Recovery = 151%  Analysis Date = 06/06/15 
 Pct Recovery = 154%  Analysis Date = 06/06/15 
 Pct Recovery = 154%  Analysis Date = 06/02/15 
 Pct Recovery = 157%  Analysis Date = 06/02/15 
 Pct Recovery = 157%  Analysis Date = 05/29/15 
 Pct Recovery = 159%  Analysis Date = 05/29/15 
 Pct Recovery = 159%  Analysis Date = 05/25/15 
 Pct Recovery = 162%  Analysis Date = 05/25/15 
 Pct Recovery = 162%  Analysis Date = 05/21/15 
 Pct Recovery = 165%  Analysis Date = 05/21/15 
 Pct Recovery = 165%  Analysis Date = 05/17/15 
 Pct Recovery = 168%  Analysis Date = 05/17/15 
 Pct Recovery = 168%  Analysis Date = 05/13/15 
 Pct Recovery = 172%  Analysis Date = 05/13/15 
 Pct Recovery = 172%  Analysis Date = 05/09/15 
 Pct Recovery = 177%  Analysis Date = 05/09/15 
 Pct Recovery = 177%  Analysis Date = 05/05/15 
 Pct Recovery = 181%  Analysis Date = 05/05/15 
 Pct Recovery = 181%  Analysis Date = 04/30/15 
 Pct Recovery = 183%  Analysis Date = 04/30/15 
 Pct Recovery = 183%  Analysis Date = 04/26/15 
 Pct Recovery = 184%  Analysis Date = 04/26/15 
 Pct Recovery = 184%  Analysis Date = 04/22/15 
 Pct Recovery = 186%  Analysis Date = 04/22/15 
 Pct Recovery = 186%  Analysis Date = 04/18/15 
 Pct Recovery = 188%  Analysis Date = 04/18/15 
 Pct Recovery = 188%  Analysis Date = 04/14/15 
 Pct Recovery = 190%  Analysis Date = 04/14/15 
 Pct Recovery = 190%  Analysis Date = 04/10/15 
 Pct Recovery = 191%  Analysis Date = 04/10/15 
 Pct Recovery = 191%  Analysis Date = 04/06/15 
 Pct Recovery = 193%  Analysis Date = 04/06/15 
 Pct Recovery = 193%  Analysis Date = 04/02/15 
 Pct Recovery = 195%  Analysis Date = 04/02/15 
 Pct Recovery = 195%  Analysis Date = 03/29/15 
 Pct Recovery = 197%  Analysis Date = 03/29/15 
 Pct Recovery = 197%  Analysis Date = 03/25/15 
 Pct Recovery = 198%  Analysis Date = 03/25/15 
 Pct Recovery = 198%  Analysis Date = 03/21/15 
 Pct Recovery = 200%  Analysis Date = 03/21/15 
 Pct Recovery = 200%  Analysis Date = 03/17/15 
 Pct Recovery = 202%  Analysis Date = 03/17/15 
 Pct Recovery = 202%  Analysis Date = 03/13/15 
 Pct Recovery = 204%  Analysis Date = 03/13/15 
 Pct Recovery = 204%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
ACETATE, ETHYL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 35 180% 191% 106% 43%
Total 35 180% 191% 106% 43%

Sample Statistics
ACETATE, ETHYL

Characteristic N % % Basis
Plotted 35 97% Spiked
Estimated Values 3 8% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 36 .  
False Negatives 1 3% 1 out of 36
Not Spiked 19 .  
False Positives 8 42% 8 out of 19

BQS OBSP Determination:
ACETATE, ISOBUTYL
METHOD: 4437 , TESTIDCODE: 77201GM016
Open Data Set

 Analysis Date = 07/29/16 
 SpikeMix = Supelco LC20145V: 40 µl & NSI 041516: 40 µl & NSI 041416HVOC: 40 µl 
 Pct Recovery = 104%  Analysis Date = 07/06/16 
 SpikeMix = Accu 216041354: 40 µl & NSI 041516: 40 µl & NSI 041416HVOC: 40 µl 
 Pct Recovery = 121%  Analysis Date = 08/13/14 
 SpikeMix = ERA 0321-14-05: 20 µl & Accu 214031128: 20 µl 
 Pct Recovery = 120%  Analysis Date = 07/23/14 
 SpikeMix = Accu 214031128: 20 µl & Abs 032014: 20 µl 
 Pct Recovery = 89%  Analysis Date = 07/11/14 
 SpikeMix = ChemService 2615700: 20 µl & Accu 214031128: 20 µl 
 Pct Recovery = 112%  Analysis Date = 05/07/14 
 SpikeMix = NSI 031814: 20 µl & Accu 214031128: 20 µl 
 Pct Recovery = 71%  Analysis Date = 08/11/16 
 SpikeMix = Phenova B20160303: 25 µl & Supelco LC20145V: 25 µl & NSI 041416HVOC: 25 µl 
 Pct Recovery = 78%  Analysis Date = 07/14/16 
 SpikeMix = NSI 041516: 25 µl & ChemService 5082800: 25 µl & NSI 041416HVOC: 25 µl 
 Pct Recovery = 112%  Analysis Date = 05/21/16 
 SpikeMix = Supelco LC20145V: 25 µl & NSI 041516: 25 µl & NSI 041416HVOC: 25 µl 
 Pct Recovery = 123%  Analysis Date = 03/19/15 
 SpikeMix = Supelco LC06437: 20 µl & NSI 031814: 20 µl 
 Pct Recovery = 142%  Analysis Date = 08/20/14 
 SpikeMix = Supelco LC06437: 20 µl & Abs 032014: 20 µl 
 Pct Recovery = 124%  Analysis Date = 06/07/14 
 SpikeMix = ChemService 2615700: 20 µl & Supelco LC06437: 20 µl 
 Pct Recovery = 105%  Analysis Date = 01/22/16 
 SpikeMix = NSI 050515HVOC: 25 µl & ERA 0601-15-05: 25 µl 
 Pct Recovery = 88%  Analysis Date = 10/09/15 
 SpikeMix = Supelco LC13544: 25 µl & NSI 050515HVOC: 25 µl 
 Pct Recovery = 96%  Analysis Date = 06/25/15 
 SpikeMix = ChemService 3818700: 25 µl & NSI 050515HVOC: 25 µl 
 Pct Recovery = 72%  Analysis Date = 07/06/16 
 SpikeMix = Phenova B20160303: 15 µl & Accu 216041354: 15 µl & NSI 041416HVOC: 15 µl 
 Pct Recovery = 68%  Analysis Date = 06/03/16 
 SpikeMix = NSI 041516: 15 µl & Phenova B20160303: 15 µl & NSI 041416HVOC: 15 µl 
 Pct Recovery = 109%  Analysis Date = 07/27/16 
 SpikeMix = ChemService 5082800: 15 µl & Supelco LC20145V: 15 µl & Accu 216041225: 15 µl 
 Pct Recovery = 87%  Analysis Date = 05/20/16 
 SpikeMix = Accu 216041354: 15 µl & NSI 041516: 15 µl & Accu 216041225: 15 µl 
 Pct Recovery = 117%  Analysis Date = 11/25/15 
 SpikeMix = Accu 215041338: 15 µl & Abs 040315: 15 µl 
 Pct Recovery = 103%  Analysis Date = 09/24/15 
 SpikeMix = Abs 040315: 15 µl & ERA 0601-15-05: 15 µl 
 Pct Recovery = 88%  Analysis Date = 09/05/15 
 SpikeMix = Accu 215041338: 15 µl & NSI 050515HVOC: 15 µl 
 Pct Recovery = 84%  Analysis Date = 07/30/15 
 SpikeMix = Supelco LC13544: 15 µl & NSI 050515HVOC: 15 µl 
 Pct Recovery = 79%  Analysis Date = 06/16/15 
 SpikeMix = ChemService 3818700: 15 µl & NSI 050515HVOC: 15 µl 
 Pct Recovery = 80%  Analysis Date = 12/13/14 
 SpikeMix = Accu 214031128: 10 µl & NSI 031814: 10 µl 
 Pct Recovery = 99%  Analysis Date = 10/21/14 
 SpikeMix = ERA 0321-14-05A: 10 µl & Accu 214031128: 10 µl 
 Pct Recovery = 133%  Analysis Date = 09/11/14 
 SpikeMix = Accu 214031128: 10 µl & Abs 032014: 10 µl 
 Pct Recovery = 92%  Analysis Date = 05/20/14 
 SpikeMix = ChemService 2615700: 10 µl & Accu 214031128: 10 µl 
 Pct Recovery = 113%  Analysis Date = 11/22/14 
 SpikeMix = ChemService 2615700: 10 µl & Supelco LC06437: 10 µl 
 Pct Recovery = 131%  Analysis Date = 09/06/14 
 SpikeMix = ERA 0321-14-05: 10 µl & Supelco LC06437: 10 µl 
 Pct Recovery = 156%  Analysis Date = 06/17/14 
 SpikeMix = Supelco LC06437: 10 µl & Abs 032014: 10 µl 
 Pct Recovery = 131%  Analysis Date = 04/09/16 
 SpikeMix = Abs 040315: 10 µl & ChemService 3818700: 10 µl 
 Pct Recovery = 101%  Analysis Date = 03/22/16 
 SpikeMix = Supelco LC13544: 10 µl & NSI 050515HVOC: 10 µl 
 Pct Recovery = 93%  Analysis Date = 01/05/16 
 SpikeMix = Accu 215041338: 10 µl & Abs 040315: 10 µl 
 Pct Recovery = 107%  Analysis Date = 12/05/15 
 SpikeMix = NSI 050515HVOC: 10 µl & ERA 0601-15-05: 10 µl 
 Pct Recovery = 84%  Analysis Date = 10/23/15 
 SpikeMix = Abs 040315: 10 µl & ChemService 3818700: 10 µl 
 Pct Recovery = 100%  Analysis Date = 08/14/15 
 SpikeMix = Abs 040315: 10 µl & ERA 0601-15-05: 10 µl 
 Pct Recovery = 72%  Analysis Date = 05/05/15 
 SpikeMix = Supelco LC13544: 10 µl & Abs 040315: 10 µl 
 Pct Recovery = 103%  Analysis Date = 08/10/16 
 Pct Recovery = 101%  Analysis Date = 08/06/16 
 Pct Recovery = 101%  Analysis Date = 08/06/16 
 Pct Recovery = 101%  Analysis Date = 08/02/16 
 Pct Recovery = 101%  Analysis Date = 08/02/16 
 Pct Recovery = 101%  Analysis Date = 07/29/16 
 Pct Recovery = 101%  Analysis Date = 07/29/16 
 Pct Recovery = 101%  Analysis Date = 07/25/16 
 Pct Recovery = 100%  Analysis Date = 07/25/16 
 Pct Recovery = 100%  Analysis Date = 07/21/16 
 Pct Recovery = 100%  Analysis Date = 07/21/16 
 Pct Recovery = 100%  Analysis Date = 07/17/16 
 Pct Recovery = 100%  Analysis Date = 07/17/16 
 Pct Recovery = 100%  Analysis Date = 07/13/16 
 Pct Recovery = 100%  Analysis Date = 07/13/16 
 Pct Recovery = 100%  Analysis Date = 07/08/16 
 Pct Recovery = 100%  Analysis Date = 07/08/16 
 Pct Recovery = 100%  Analysis Date = 07/04/16 
 Pct Recovery = 100%  Analysis Date = 07/04/16 
 Pct Recovery = 100%  Analysis Date = 06/30/16 
 Pct Recovery = 100%  Analysis Date = 06/30/16 
 Pct Recovery = 100%  Analysis Date = 06/26/16 
 Pct Recovery = 100%  Analysis Date = 06/26/16 
 Pct Recovery = 100%  Analysis Date = 06/22/16 
 Pct Recovery = 100%  Analysis Date = 06/22/16 
 Pct Recovery = 100%  Analysis Date = 06/18/16 
 Pct Recovery = 100%  Analysis Date = 06/18/16 
 Pct Recovery = 100%  Analysis Date = 06/14/16 
 Pct Recovery = 100%  Analysis Date = 06/14/16 
 Pct Recovery = 100%  Analysis Date = 06/09/16 
 Pct Recovery = 100%  Analysis Date = 06/09/16 
 Pct Recovery = 100%  Analysis Date = 06/05/16 
 Pct Recovery = 100%  Analysis Date = 06/05/16 
 Pct Recovery = 100%  Analysis Date = 06/01/16 
 Pct Recovery = 100%  Analysis Date = 06/01/16 
 Pct Recovery = 100%  Analysis Date = 05/28/16 
 Pct Recovery = 100%  Analysis Date = 05/28/16 
 Pct Recovery = 100%  Analysis Date = 05/24/16 
 Pct Recovery = 100%  Analysis Date = 05/24/16 
 Pct Recovery = 100%  Analysis Date = 05/20/16 
 Pct Recovery = 100%  Analysis Date = 05/20/16 
 Pct Recovery = 100%  Analysis Date = 05/16/16 
 Pct Recovery = 100%  Analysis Date = 05/16/16 
 Pct Recovery = 100%  Analysis Date = 05/12/16 
 Pct Recovery = 100%  Analysis Date = 05/12/16 
 Pct Recovery = 100%  Analysis Date = 05/07/16 
 Pct Recovery = 100%  Analysis Date = 05/07/16 
 Pct Recovery = 100%  Analysis Date = 05/03/16 
 Pct Recovery = 100%  Analysis Date = 05/03/16 
 Pct Recovery = 100%  Analysis Date = 04/29/16 
 Pct Recovery = 100%  Analysis Date = 04/29/16 
 Pct Recovery = 100%  Analysis Date = 04/25/16 
 Pct Recovery = 100%  Analysis Date = 04/25/16 
 Pct Recovery = 100%  Analysis Date = 04/21/16 
 Pct Recovery = 100%  Analysis Date = 04/21/16 
 Pct Recovery = 100%  Analysis Date = 04/17/16 
 Pct Recovery = 100%  Analysis Date = 04/17/16 
 Pct Recovery = 100%  Analysis Date = 04/13/16 
 Pct Recovery = 100%  Analysis Date = 04/13/16 
 Pct Recovery = 100%  Analysis Date = 04/08/16 
 Pct Recovery = 99%  Analysis Date = 04/08/16 
 Pct Recovery = 99%  Analysis Date = 04/04/16 
 Pct Recovery = 99%  Analysis Date = 04/04/16 
 Pct Recovery = 99%  Analysis Date = 03/31/16 
 Pct Recovery = 99%  Analysis Date = 03/31/16 
 Pct Recovery = 99%  Analysis Date = 03/27/16 
 Pct Recovery = 99%  Analysis Date = 03/27/16 
 Pct Recovery = 99%  Analysis Date = 03/23/16 
 Pct Recovery = 99%  Analysis Date = 03/23/16 
 Pct Recovery = 99%  Analysis Date = 03/19/16 
 Pct Recovery = 99%  Analysis Date = 03/19/16 
 Pct Recovery = 99%  Analysis Date = 03/15/16 
 Pct Recovery = 99%  Analysis Date = 03/15/16 
 Pct Recovery = 99%  Analysis Date = 03/11/16 
 Pct Recovery = 99%  Analysis Date = 03/11/16 
 Pct Recovery = 99%  Analysis Date = 03/06/16 
 Pct Recovery = 99%  Analysis Date = 03/06/16 
 Pct Recovery = 99%  Analysis Date = 03/02/16 
 Pct Recovery = 99%  Analysis Date = 03/02/16 
 Pct Recovery = 99%  Analysis Date = 02/27/16 
 Pct Recovery = 99%  Analysis Date = 02/27/16 
 Pct Recovery = 99%  Analysis Date = 02/23/16 
 Pct Recovery = 99%  Analysis Date = 02/23/16 
 Pct Recovery = 99%  Analysis Date = 02/19/16 
 Pct Recovery = 99%  Analysis Date = 02/19/16 
 Pct Recovery = 99%  Analysis Date = 02/15/16 
 Pct Recovery = 99%  Analysis Date = 02/15/16 
 Pct Recovery = 99%  Analysis Date = 02/11/16 
 Pct Recovery = 99%  Analysis Date = 02/11/16 
 Pct Recovery = 99%  Analysis Date = 02/06/16 
 Pct Recovery = 99%  Analysis Date = 02/06/16 
 Pct Recovery = 99%  Analysis Date = 02/02/16 
 Pct Recovery = 99%  Analysis Date = 02/02/16 
 Pct Recovery = 99%  Analysis Date = 01/29/16 
 Pct Recovery = 98%  Analysis Date = 01/29/16 
 Pct Recovery = 98%  Analysis Date = 01/25/16 
 Pct Recovery = 98%  Analysis Date = 01/25/16 
 Pct Recovery = 98%  Analysis Date = 01/21/16 
 Pct Recovery = 98%  Analysis Date = 01/21/16 
 Pct Recovery = 98%  Analysis Date = 01/17/16 
 Pct Recovery = 98%  Analysis Date = 01/17/16 
 Pct Recovery = 98%  Analysis Date = 01/13/16 
 Pct Recovery = 98%  Analysis Date = 01/13/16 
 Pct Recovery = 98%  Analysis Date = 01/08/16 
 Pct Recovery = 97%  Analysis Date = 01/08/16 
 Pct Recovery = 97%  Analysis Date = 01/04/16 
 Pct Recovery = 97%  Analysis Date = 01/04/16 
 Pct Recovery = 97%  Analysis Date = 12/31/15 
 Pct Recovery = 96%  Analysis Date = 12/31/15 
 Pct Recovery = 96%  Analysis Date = 12/27/15 
 Pct Recovery = 96%  Analysis Date = 12/27/15 
 Pct Recovery = 96%  Analysis Date = 12/23/15 
 Pct Recovery = 96%  Analysis Date = 12/23/15 
 Pct Recovery = 96%  Analysis Date = 12/19/15 
 Pct Recovery = 95%  Analysis Date = 12/19/15 
 Pct Recovery = 95%  Analysis Date = 12/15/15 
 Pct Recovery = 95%  Analysis Date = 12/15/15 
 Pct Recovery = 95%  Analysis Date = 12/11/15 
 Pct Recovery = 94%  Analysis Date = 12/11/15 
 Pct Recovery = 94%  Analysis Date = 12/06/15 
 Pct Recovery = 94%  Analysis Date = 12/06/15 
 Pct Recovery = 94%  Analysis Date = 12/02/15 
 Pct Recovery = 94%  Analysis Date = 12/02/15 
 Pct Recovery = 94%  Analysis Date = 11/28/15 
 Pct Recovery = 93%  Analysis Date = 11/28/15 
 Pct Recovery = 93%  Analysis Date = 11/24/15 
 Pct Recovery = 93%  Analysis Date = 11/24/15 
 Pct Recovery = 93%  Analysis Date = 11/20/15 
 Pct Recovery = 93%  Analysis Date = 11/20/15 
 Pct Recovery = 93%  Analysis Date = 11/16/15 
 Pct Recovery = 93%  Analysis Date = 11/16/15 
 Pct Recovery = 93%  Analysis Date = 11/12/15 
 Pct Recovery = 92%  Analysis Date = 11/12/15 
 Pct Recovery = 92%  Analysis Date = 11/07/15 
 Pct Recovery = 92%  Analysis Date = 11/07/15 
 Pct Recovery = 92%  Analysis Date = 11/03/15 
 Pct Recovery = 92%  Analysis Date = 11/03/15 
 Pct Recovery = 92%  Analysis Date = 10/30/15 
 Pct Recovery = 92%  Analysis Date = 10/30/15 
 Pct Recovery = 92%  Analysis Date = 10/26/15 
 Pct Recovery = 92%  Analysis Date = 10/26/15 
 Pct Recovery = 92%  Analysis Date = 10/22/15 
 Pct Recovery = 91%  Analysis Date = 10/22/15 
 Pct Recovery = 91%  Analysis Date = 10/18/15 
 Pct Recovery = 91%  Analysis Date = 10/18/15 
 Pct Recovery = 91%  Analysis Date = 10/14/15 
 Pct Recovery = 91%  Analysis Date = 10/14/15 
 Pct Recovery = 91%  Analysis Date = 10/10/15 
 Pct Recovery = 91%  Analysis Date = 10/10/15 
 Pct Recovery = 91%  Analysis Date = 10/05/15 
 Pct Recovery = 91%  Analysis Date = 10/05/15 
 Pct Recovery = 91%  Analysis Date = 10/01/15 
 Pct Recovery = 91%  Analysis Date = 10/01/15 
 Pct Recovery = 91%  Analysis Date = 09/27/15 
 Pct Recovery = 91%  Analysis Date = 09/27/15 
 Pct Recovery = 91%  Analysis Date = 09/23/15 
 Pct Recovery = 91%  Analysis Date = 09/23/15 
 Pct Recovery = 91%  Analysis Date = 09/19/15 
 Pct Recovery = 91%  Analysis Date = 09/19/15 
 Pct Recovery = 91%  Analysis Date = 09/15/15 
 Pct Recovery = 91%  Analysis Date = 09/15/15 
 Pct Recovery = 91%  Analysis Date = 09/11/15 
 Pct Recovery = 91%  Analysis Date = 09/11/15 
 Pct Recovery = 91%  Analysis Date = 09/06/15 
 Pct Recovery = 92%  Analysis Date = 09/06/15 
 Pct Recovery = 92%  Analysis Date = 09/02/15 
 Pct Recovery = 92%  Analysis Date = 09/02/15 
 Pct Recovery = 92%  Analysis Date = 08/29/15 
 Pct Recovery = 92%  Analysis Date = 08/29/15 
 Pct Recovery = 92%  Analysis Date = 08/25/15 
 Pct Recovery = 92%  Analysis Date = 08/25/15 
 Pct Recovery = 92%  Analysis Date = 08/21/15 
 Pct Recovery = 92%  Analysis Date = 08/21/15 
 Pct Recovery = 92%  Analysis Date = 08/17/15 
 Pct Recovery = 92%  Analysis Date = 08/17/15 
 Pct Recovery = 92%  Analysis Date = 08/13/15 
 Pct Recovery = 92%  Analysis Date = 08/13/15 
 Pct Recovery = 92%  Analysis Date = 08/08/15 
 Pct Recovery = 92%  Analysis Date = 08/08/15 
 Pct Recovery = 92%  Analysis Date = 08/04/15 
 Pct Recovery = 93%  Analysis Date = 08/04/15 
 Pct Recovery = 93%  Analysis Date = 07/31/15 
 Pct Recovery = 93%  Analysis Date = 07/31/15 
 Pct Recovery = 93%  Analysis Date = 07/27/15 
 Pct Recovery = 94%  Analysis Date = 07/27/15 
 Pct Recovery = 94%  Analysis Date = 07/23/15 
 Pct Recovery = 94%  Analysis Date = 07/23/15 
 Pct Recovery = 94%  Analysis Date = 07/19/15 
 Pct Recovery = 94%  Analysis Date = 07/19/15 
 Pct Recovery = 94%  Analysis Date = 07/15/15 
 Pct Recovery = 95%  Analysis Date = 07/15/15 
 Pct Recovery = 95%  Analysis Date = 07/11/15 
 Pct Recovery = 95%  Analysis Date = 07/11/15 
 Pct Recovery = 95%  Analysis Date = 07/06/15 
 Pct Recovery = 95%  Analysis Date = 07/06/15 
 Pct Recovery = 95%  Analysis Date = 07/02/15 
 Pct Recovery = 96%  Analysis Date = 07/02/15 
 Pct Recovery = 96%  Analysis Date = 06/28/15 
 Pct Recovery = 96%  Analysis Date = 06/28/15 
 Pct Recovery = 96%  Analysis Date = 06/24/15 
 Pct Recovery = 96%  Analysis Date = 06/24/15 
 Pct Recovery = 96%  Analysis Date = 06/20/15 
 Pct Recovery = 97%  Analysis Date = 06/20/15 
 Pct Recovery = 97%  Analysis Date = 06/16/15 
 Pct Recovery = 97%  Analysis Date = 06/16/15 
 Pct Recovery = 97%  Analysis Date = 06/12/15 
 Pct Recovery = 97%  Analysis Date = 06/12/15 
 Pct Recovery = 97%  Analysis Date = 06/07/15 
 Pct Recovery = 98%  Analysis Date = 06/07/15 
 Pct Recovery = 98%  Analysis Date = 06/03/15 
 Pct Recovery = 98%  Analysis Date = 06/03/15 
 Pct Recovery = 98%  Analysis Date = 05/30/15 
 Pct Recovery = 98%  Analysis Date = 05/30/15 
 Pct Recovery = 98%  Analysis Date = 05/26/15 
 Pct Recovery = 99%  Analysis Date = 05/26/15 
 Pct Recovery = 99%  Analysis Date = 05/22/15 
 Pct Recovery = 99%  Analysis Date = 05/22/15 
 Pct Recovery = 99%  Analysis Date = 05/18/15 
 Pct Recovery = 99%  Analysis Date = 05/18/15 
 Pct Recovery = 99%  Analysis Date = 05/14/15 
 Pct Recovery = 100%  Analysis Date = 05/14/15 
 Pct Recovery = 100%  Analysis Date = 05/10/15 
 Pct Recovery = 100%  Analysis Date = 05/10/15 
 Pct Recovery = 100%  Analysis Date = 05/05/15 
 Pct Recovery = 101%  Analysis Date = 05/05/15 
 Pct Recovery = 101%  Analysis Date = 05/01/15 
 Pct Recovery = 101%  Analysis Date = 05/01/15 
 Pct Recovery = 101%  Analysis Date = 04/27/15 
 Pct Recovery = 101%  Analysis Date = 04/27/15 
 Pct Recovery = 101%  Analysis Date = 04/23/15 
 Pct Recovery = 102%  Analysis Date = 04/23/15 
 Pct Recovery = 102%  Analysis Date = 04/19/15 
 Pct Recovery = 102%  Analysis Date = 04/19/15 
 Pct Recovery = 102%  Analysis Date = 04/15/15 
 Pct Recovery = 102%  Analysis Date = 04/15/15 
 Pct Recovery = 102%  Analysis Date = 04/11/15 
 Pct Recovery = 103%  Analysis Date = 04/11/15 
 Pct Recovery = 103%  Analysis Date = 04/06/15 
 Pct Recovery = 103%  Analysis Date = 04/06/15 
 Pct Recovery = 103%  Analysis Date = 04/02/15 
 Pct Recovery = 103%  Analysis Date = 04/02/15 
 Pct Recovery = 103%  Analysis Date = 03/29/15 
 Pct Recovery = 104%  Analysis Date = 03/29/15 
 Pct Recovery = 104%  Analysis Date = 03/25/15 
 Pct Recovery = 104%  Analysis Date = 03/25/15 
 Pct Recovery = 104%  Analysis Date = 03/21/15 
 Pct Recovery = 104%  Analysis Date = 03/21/15 
 Pct Recovery = 104%  Analysis Date = 03/17/15 
 Pct Recovery = 105%  Analysis Date = 03/17/15 
 Pct Recovery = 105%  Analysis Date = 03/13/15 
 Pct Recovery = 105%  Analysis Date = 03/13/15 
 Pct Recovery = 105%  Analysis Date = 03/08/15 
 Pct Recovery = 105%  Analysis Date = 03/08/15 
 Pct Recovery = 105%  Analysis Date = 03/04/15 
 Pct Recovery = 106%  Analysis Date = 03/04/15 
 Pct Recovery = 106%  Analysis Date = 02/28/15 
 Pct Recovery = 106%  Analysis Date = 02/28/15 
 Pct Recovery = 106%  Analysis Date = 02/24/15 
 Pct Recovery = 106%  Analysis Date = 02/24/15 
 Pct Recovery = 106%  Analysis Date = 02/20/15 
 Pct Recovery = 107%  Analysis Date = 02/20/15 
 Pct Recovery = 107%  Analysis Date = 02/16/15 
 Pct Recovery = 107%  Analysis Date = 02/16/15 
 Pct Recovery = 107%  Analysis Date = 02/12/15 
 Pct Recovery = 107%  Analysis Date = 02/12/15 
 Pct Recovery = 107%  Analysis Date = 02/08/15 
 Pct Recovery = 108%  Analysis Date = 02/08/15 
 Pct Recovery = 108%  Analysis Date = 02/03/15 
 Pct Recovery = 108%  Analysis Date = 02/03/15 
 Pct Recovery = 108%  Analysis Date = 01/30/15 
 Pct Recovery = 108%  Analysis Date = 01/30/15 
 Pct Recovery = 108%  Analysis Date = 01/26/15 
 Pct Recovery = 109%  Analysis Date = 01/26/15 
 Pct Recovery = 109%  Analysis Date = 01/22/15 
 Pct Recovery = 109%  Analysis Date = 01/22/15 
 Pct Recovery = 109%  Analysis Date = 01/18/15 
 Pct Recovery = 109%  Analysis Date = 01/18/15 
 Pct Recovery = 109%  Analysis Date = 01/14/15 
 Pct Recovery = 110%  Analysis Date = 01/14/15 
 Pct Recovery = 110%  Analysis Date = 01/10/15 
 Pct Recovery = 110%  Analysis Date = 01/10/15 
 Pct Recovery = 110%  Analysis Date = 01/05/15 
 Pct Recovery = 110%  Analysis Date = 01/05/15 
 Pct Recovery = 110%  Analysis Date = 01/01/15 
 Pct Recovery = 111%  Analysis Date = 01/01/15 
 Pct Recovery = 111%  Analysis Date = 12/28/14 
 Pct Recovery = 111%  Analysis Date = 12/28/14 
 Pct Recovery = 111%  Analysis Date = 12/24/14 
 Pct Recovery = 111%  Analysis Date = 12/24/14 
 Pct Recovery = 111%  Analysis Date = 12/20/14 
 Pct Recovery = 112%  Analysis Date = 12/20/14 
 Pct Recovery = 112%  Analysis Date = 12/16/14 
 Pct Recovery = 112%  Analysis Date = 12/16/14 
 Pct Recovery = 112%  Analysis Date = 12/12/14 
 Pct Recovery = 112%  Analysis Date = 12/12/14 
 Pct Recovery = 112%  Analysis Date = 12/08/14 
 Pct Recovery = 112%  Analysis Date = 12/08/14 
 Pct Recovery = 112%  Analysis Date = 12/03/14 
 Pct Recovery = 112%  Analysis Date = 12/03/14 
 Pct Recovery = 112%  Analysis Date = 11/29/14 
 Pct Recovery = 112%  Analysis Date = 11/29/14 
 Pct Recovery = 112%  Analysis Date = 11/25/14 
 Pct Recovery = 112%  Analysis Date = 11/25/14 
 Pct Recovery = 112%  Analysis Date = 11/21/14 
 Pct Recovery = 113%  Analysis Date = 11/21/14 
 Pct Recovery = 113%  Analysis Date = 11/17/14 
 Pct Recovery = 113%  Analysis Date = 11/17/14 
 Pct Recovery = 113%  Analysis Date = 11/13/14 
 Pct Recovery = 113%  Analysis Date = 11/13/14 
 Pct Recovery = 113%  Analysis Date = 11/09/14 
 Pct Recovery = 113%  Analysis Date = 11/09/14 
 Pct Recovery = 113%  Analysis Date = 11/04/14 
 Pct Recovery = 113%  Analysis Date = 11/04/14 
 Pct Recovery = 113%  Analysis Date = 10/31/14 
 Pct Recovery = 113%  Analysis Date = 10/31/14 
 Pct Recovery = 113%  Analysis Date = 10/27/14 
 Pct Recovery = 113%  Analysis Date = 10/27/14 
 Pct Recovery = 113%  Analysis Date = 10/23/14 
 Pct Recovery = 113%  Analysis Date = 10/23/14 
 Pct Recovery = 113%  Analysis Date = 10/19/14 
 Pct Recovery = 113%  Analysis Date = 10/19/14 
 Pct Recovery = 113%  Analysis Date = 10/15/14 
 Pct Recovery = 113%  Analysis Date = 10/15/14 
 Pct Recovery = 113%  Analysis Date = 10/11/14 
 Pct Recovery = 113%  Analysis Date = 10/11/14 
 Pct Recovery = 113%  Analysis Date = 10/06/14 
 Pct Recovery = 113%  Analysis Date = 10/06/14 
 Pct Recovery = 113%  Analysis Date = 10/02/14 
 Pct Recovery = 113%  Analysis Date = 10/02/14 
 Pct Recovery = 113%  Analysis Date = 09/28/14 
 Pct Recovery = 113%  Analysis Date = 09/28/14 
 Pct Recovery = 113%  Analysis Date = 09/24/14 
 Pct Recovery = 113%  Analysis Date = 09/24/14 
 Pct Recovery = 113%  Analysis Date = 09/20/14 
 Pct Recovery = 113%  Analysis Date = 09/20/14 
 Pct Recovery = 113%  Analysis Date = 09/16/14 
 Pct Recovery = 113%  Analysis Date = 09/16/14 
 Pct Recovery = 113%  Analysis Date = 09/12/14 
 Pct Recovery = 113%  Analysis Date = 09/12/14 
 Pct Recovery = 113%  Analysis Date = 09/08/14 
 Pct Recovery = 113%  Analysis Date = 09/08/14 
 Pct Recovery = 113%  Analysis Date = 09/03/14 
 Pct Recovery = 113%  Analysis Date = 09/03/14 
 Pct Recovery = 113%  Analysis Date = 08/30/14 
 Pct Recovery = 113%  Analysis Date = 08/30/14 
 Pct Recovery = 113%  Analysis Date = 08/26/14 
 Pct Recovery = 113%  Analysis Date = 08/26/14 
 Pct Recovery = 113%  Analysis Date = 08/22/14 
 Pct Recovery = 113%  Analysis Date = 08/22/14 
 Pct Recovery = 113%  Analysis Date = 08/18/14 
 Pct Recovery = 113%  Analysis Date = 08/18/14 
 Pct Recovery = 113%  Analysis Date = 08/14/14 
 Pct Recovery = 113%  Analysis Date = 08/14/14 
 Pct Recovery = 113%  Analysis Date = 08/10/14 
 Pct Recovery = 113%  Analysis Date = 08/10/14 
 Pct Recovery = 113%  Analysis Date = 08/05/14 
 Pct Recovery = 112%  Analysis Date = 08/05/14 
 Pct Recovery = 112%  Analysis Date = 08/01/14 
 Pct Recovery = 112%  Analysis Date = 08/01/14 
 Pct Recovery = 112%  Analysis Date = 07/28/14 
 Pct Recovery = 112%  Analysis Date = 07/28/14 
 Pct Recovery = 112%  Analysis Date = 07/24/14 
 Pct Recovery = 112%  Analysis Date = 07/24/14 
 Pct Recovery = 112%  Analysis Date = 07/20/14 
 Pct Recovery = 112%  Analysis Date = 07/20/14 
 Pct Recovery = 112%  Analysis Date = 07/16/14 
 Pct Recovery = 112%  Analysis Date = 07/16/14 
 Pct Recovery = 112%  Analysis Date = 07/12/14 
 Pct Recovery = 112%  Analysis Date = 07/12/14 
 Pct Recovery = 112%  Analysis Date = 07/08/14 
 Pct Recovery = 112%  Analysis Date = 07/08/14 
 Pct Recovery = 112%  Analysis Date = 07/03/14 
 Pct Recovery = 112%  Analysis Date = 07/03/14 
 Pct Recovery = 112%  Analysis Date = 06/29/14 
 Pct Recovery = 111%  Analysis Date = 06/29/14 
 Pct Recovery = 111%  Analysis Date = 06/25/14 
 Pct Recovery = 111%  Analysis Date = 06/25/14 
 Pct Recovery = 111%  Analysis Date = 06/21/14 
 Pct Recovery = 111%  Analysis Date = 06/21/14 
 Pct Recovery = 111%  Analysis Date = 06/17/14 
 Pct Recovery = 111%  Analysis Date = 06/17/14 
 Pct Recovery = 111%  Analysis Date = 06/13/14 
 Pct Recovery = 111%  Analysis Date = 06/13/14 
 Pct Recovery = 111%  Analysis Date = 06/09/14 
 Pct Recovery = 111%  Analysis Date = 06/09/14 
 Pct Recovery = 111%  Analysis Date = 06/04/14 
 Pct Recovery = 111%  Analysis Date = 06/04/14 
 Pct Recovery = 111%  Analysis Date = 05/31/14 
 Pct Recovery = 110%  Analysis Date = 05/31/14 
 Pct Recovery = 110%  Analysis Date = 05/27/14 
 Pct Recovery = 110%  Analysis Date = 05/27/14 
 Pct Recovery = 110%  Analysis Date = 05/23/14 
 Pct Recovery = 110%  Analysis Date = 05/23/14 
 Pct Recovery = 110%  Analysis Date = 05/19/14 
 Pct Recovery = 110%  Analysis Date = 05/19/14 
 Pct Recovery = 110%  Analysis Date = 05/15/14 
 Pct Recovery = 110%  Analysis Date = 05/15/14 
 Pct Recovery = 110%  Analysis Date = 05/11/14 
 Pct Recovery = 109%  Analysis Date = 05/11/14 
 Pct Recovery = 109%  Analysis Date = 05/07/14 
 Pct Recovery = 109%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
ACETATE, ISOBUTYL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 38 102% 21% 102% 22%
Total 38 102% 21% 102% 22%

Sample Statistics
ACETATE, ISOBUTYL

Characteristic N % % Basis
Plotted 38 100% Spiked
Estimated Values 2 5% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 38 .  
False Negatives 0 0% 0 out of 38
Not Spiked 17 .  
False Positives 1 6% 1 out of 17

BQS OBSP Determination:
ACETATE, ISOPROPYL
METHOD: 4437 , TESTIDCODE: 45013GM016
Open Data Set

 Analysis Date = 07/29/16 
 SpikeMix = Supelco LC20145V: 40 µl & NSI 041516: 40 µl & NSI 041416HVOC: 40 µl 
 Pct Recovery = 79%  Analysis Date = 07/06/16 
 SpikeMix = Accu 216041354: 40 µl & NSI 041516: 40 µl & NSI 041416HVOC: 40 µl 
 Pct Recovery = 72%  Analysis Date = 01/22/16 
 SpikeMix = NSI 050515HVOC: 25 µl & ERA 0601-15-05: 25 µl 
 Pct Recovery = 104%  Analysis Date = 10/09/15 
 SpikeMix = ERA 0601-15-05: 25 µl & Accu 215041338: 25 µl 
 Pct Recovery = 83%  Analysis Date = 08/11/16 
 SpikeMix = Phenova B20160303: 25 µl & Supelco LC20145V: 25 µl & NSI 041416HVOC: 25 µl 
 Pct Recovery = 76%  Analysis Date = 07/14/16 
 SpikeMix = NSI 041516: 25 µl & ChemService 5082800: 25 µl & NSI 041416HVOC: 25 µl 
 Pct Recovery = 86%  Analysis Date = 05/26/16 
 SpikeMix = Supelco LC20145V: 25 µl & NSI 041516: 25 µl & NSI 041416HVOC: 25 µl 
 Pct Recovery = 76%  Analysis Date = 03/19/15 
 SpikeMix = Supelco LC06437: 20 µl & NSI 031814: 20 µl 
 Pct Recovery = 136%  Analysis Date = 01/10/15 
 SpikeMix = Abs 032014: 20 µl & ERA 0321-14-05A: 20 µl 
 Pct Recovery = 107%  Analysis Date = 08/20/14 
 SpikeMix = Supelco LC06437: 20 µl & Abs 032014: 20 µl 
 Pct Recovery = 116%  Analysis Date = 07/23/14 
 SpikeMix = Accu 214031128: 20 µl & Abs 032014: 20 µl 
 Pct Recovery = 112%  Analysis Date = 07/03/14 
 SpikeMix = Abs 032014: 20 µl & ChemService 2615700: 20 µl 
 Pct Recovery = 107%  Analysis Date = 06/06/14 
 SpikeMix = NSI 031814: 20 µl & ChemService 2615700: 20 µl 
 Pct Recovery = 105%  Analysis Date = 05/07/14 
 SpikeMix = NSI 031814: 20 µl & Accu 214031128: 20 µl 
 Pct Recovery = 103%  Analysis Date = 06/26/15 
 SpikeMix = ChemService 3818700: 25 µl & Accu 215041338: 25 µl 
 Pct Recovery = 111%  Analysis Date = 06/25/15 
 SpikeMix = ChemService 3818700: 25 µl & NSI 050515HVOC: 25 µl 
 Pct Recovery = 96%  Analysis Date = 09/24/15 
 SpikeMix = Abs 040315: 15 µl & ERA 0601-15-05: 15 µl 
 Pct Recovery = 96%  Analysis Date = 08/24/15 
 SpikeMix = ERA 0601-15-05: 15 µl & Supelco LC13544: 15 µl 
 Pct Recovery = 79%  Analysis Date = 07/06/16 
 SpikeMix = Phenova B20160303: 15 µl & Accu 216041354: 15 µl & NSI 041416HVOC: 15 µl 
 Pct Recovery = 67%  Analysis Date = 06/03/16 
 SpikeMix = NSI 041516: 15 µl & Phenova B20160303: 15 µl & NSI 041416HVOC: 15 µl 
 Pct Recovery = 96%  Analysis Date = 07/27/16 
 SpikeMix = ChemService 5082800: 15 µl & Supelco LC20145V: 15 µl & Accu 216041225: 15 µl 
 Pct Recovery = 85%  Analysis Date = 05/26/16 
 SpikeMix = Accu 216041354: 15 µl & NSI 041516: 15 µl & Accu 216041225: 15 µl 
 Pct Recovery = 83%  Analysis Date = 04/28/16 
 SpikeMix = ChemService 3818700: 15 µl & Supelco LC13544: 15 µl 
 Pct Recovery = 99%  Analysis Date = 06/16/15 
 SpikeMix = ChemService 3818700: 15 µl & NSI 050515HVOC: 15 µl 
 Pct Recovery = 95%  Analysis Date = 05/14/15 
 SpikeMix = ChemService 3818700: 15 µl & Supelco LC13544: 15 µl 
 Pct Recovery = 108%  Analysis Date = 04/25/15 
 SpikeMix = Abs 032014: 10 µl & ERA 0321-14-05A: 10 µl 
 Pct Recovery = 98%  Analysis Date = 12/13/14 
 SpikeMix = Accu 214031128: 10 µl & NSI 031814: 10 µl 
 Pct Recovery = 119%  Analysis Date = 09/11/14 
 SpikeMix = Accu 214031128: 10 µl & Abs 032014: 10 µl 
 Pct Recovery = 109%  Analysis Date = 07/30/14 
 SpikeMix = NSI 031814: 10 µl & ChemService 2615700: 10 µl 
 Pct Recovery = 105%  Analysis Date = 06/17/14 
 SpikeMix = Supelco LC06437: 10 µl & Abs 032014: 10 µl 
 Pct Recovery = 121%  Analysis Date = 02/12/16 
 SpikeMix = ERA 0601-15-05: 10 µl & Accu 215041338: 10 µl 
 Pct Recovery = 104%  Analysis Date = 12/05/15 
 SpikeMix = NSI 050515HVOC: 10 µl & ERA 0601-15-05: 10 µl 
 Pct Recovery = 88%  Analysis Date = 11/14/15 
 SpikeMix = ERA 0601-15-05: 10 µl 
 Pct Recovery = 90%  Analysis Date = 08/14/15 
 SpikeMix = Abs 040315: 10 µl & ERA 0601-15-05: 10 µl 
 Pct Recovery = 85%  Analysis Date = 04/09/16 
 SpikeMix = Abs 040315: 10 µl & ChemService 3818700: 10 µl 
 Pct Recovery = 108%  Analysis Date = 12/10/15 
 SpikeMix = ChemService 3818700: 10 µl & Supelco LC13544: 10 µl 
 Pct Recovery = 97%  Analysis Date = 10/23/15 
 SpikeMix = Abs 040315: 10 µl & ChemService 3818700: 10 µl 
 Pct Recovery = 106%  Analysis Date = 05/20/15 
 SpikeMix = ChemService 3818700: 10 µl & Accu 215041338: 10 µl 
 Pct Recovery = 115%  Analysis Date = 08/10/16 
 Pct Recovery = 80%  Analysis Date = 08/06/16 
 Pct Recovery = 80%  Analysis Date = 08/06/16 
 Pct Recovery = 80%  Analysis Date = 08/02/16 
 Pct Recovery = 80%  Analysis Date = 08/02/16 
 Pct Recovery = 80%  Analysis Date = 07/29/16 
 Pct Recovery = 81%  Analysis Date = 07/29/16 
 Pct Recovery = 81%  Analysis Date = 07/25/16 
 Pct Recovery = 81%  Analysis Date = 07/25/16 
 Pct Recovery = 81%  Analysis Date = 07/21/16 
 Pct Recovery = 81%  Analysis Date = 07/21/16 
 Pct Recovery = 81%  Analysis Date = 07/17/16 
 Pct Recovery = 82%  Analysis Date = 07/17/16 
 Pct Recovery = 82%  Analysis Date = 07/13/16 
 Pct Recovery = 82%  Analysis Date = 07/13/16 
 Pct Recovery = 82%  Analysis Date = 07/08/16 
 Pct Recovery = 82%  Analysis Date = 07/08/16 
 Pct Recovery = 82%  Analysis Date = 07/04/16 
 Pct Recovery = 83%  Analysis Date = 07/04/16 
 Pct Recovery = 83%  Analysis Date = 06/30/16 
 Pct Recovery = 83%  Analysis Date = 06/30/16 
 Pct Recovery = 83%  Analysis Date = 06/26/16 
 Pct Recovery = 83%  Analysis Date = 06/26/16 
 Pct Recovery = 83%  Analysis Date = 06/22/16 
 Pct Recovery = 84%  Analysis Date = 06/22/16 
 Pct Recovery = 84%  Analysis Date = 06/18/16 
 Pct Recovery = 84%  Analysis Date = 06/18/16 
 Pct Recovery = 84%  Analysis Date = 06/14/16 
 Pct Recovery = 84%  Analysis Date = 06/14/16 
 Pct Recovery = 84%  Analysis Date = 06/09/16 
 Pct Recovery = 85%  Analysis Date = 06/09/16 
 Pct Recovery = 85%  Analysis Date = 06/05/16 
 Pct Recovery = 85%  Analysis Date = 06/05/16 
 Pct Recovery = 85%  Analysis Date = 06/01/16 
 Pct Recovery = 85%  Analysis Date = 06/01/16 
 Pct Recovery = 85%  Analysis Date = 05/28/16 
 Pct Recovery = 85%  Analysis Date = 05/28/16 
 Pct Recovery = 85%  Analysis Date = 05/24/16 
 Pct Recovery = 86%  Analysis Date = 05/24/16 
 Pct Recovery = 86%  Analysis Date = 05/20/16 
 Pct Recovery = 86%  Analysis Date = 05/20/16 
 Pct Recovery = 86%  Analysis Date = 05/16/16 
 Pct Recovery = 86%  Analysis Date = 05/16/16 
 Pct Recovery = 86%  Analysis Date = 05/12/16 
 Pct Recovery = 87%  Analysis Date = 05/12/16 
 Pct Recovery = 87%  Analysis Date = 05/07/16 
 Pct Recovery = 87%  Analysis Date = 05/07/16 
 Pct Recovery = 87%  Analysis Date = 05/03/16 
 Pct Recovery = 87%  Analysis Date = 05/03/16 
 Pct Recovery = 87%  Analysis Date = 04/29/16 
 Pct Recovery = 87%  Analysis Date = 04/29/16 
 Pct Recovery = 87%  Analysis Date = 04/25/16 
 Pct Recovery = 88%  Analysis Date = 04/25/16 
 Pct Recovery = 88%  Analysis Date = 04/21/16 
 Pct Recovery = 88%  Analysis Date = 04/21/16 
 Pct Recovery = 88%  Analysis Date = 04/17/16 
 Pct Recovery = 88%  Analysis Date = 04/17/16 
 Pct Recovery = 88%  Analysis Date = 04/13/16 
 Pct Recovery = 89%  Analysis Date = 04/13/16 
 Pct Recovery = 89%  Analysis Date = 04/08/16 
 Pct Recovery = 89%  Analysis Date = 04/08/16 
 Pct Recovery = 89%  Analysis Date = 04/04/16 
 Pct Recovery = 89%  Analysis Date = 04/04/16 
 Pct Recovery = 89%  Analysis Date = 03/31/16 
 Pct Recovery = 89%  Analysis Date = 03/31/16 
 Pct Recovery = 89%  Analysis Date = 03/27/16 
 Pct Recovery = 90%  Analysis Date = 03/27/16 
 Pct Recovery = 90%  Analysis Date = 03/23/16 
 Pct Recovery = 90%  Analysis Date = 03/23/16 
 Pct Recovery = 90%  Analysis Date = 03/19/16 
 Pct Recovery = 90%  Analysis Date = 03/19/16 
 Pct Recovery = 90%  Analysis Date = 03/15/16 
 Pct Recovery = 90%  Analysis Date = 03/15/16 
 Pct Recovery = 90%  Analysis Date = 03/11/16 
 Pct Recovery = 91%  Analysis Date = 03/11/16 
 Pct Recovery = 91%  Analysis Date = 03/06/16 
 Pct Recovery = 91%  Analysis Date = 03/06/16 
 Pct Recovery = 91%  Analysis Date = 03/02/16 
 Pct Recovery = 91%  Analysis Date = 03/02/16 
 Pct Recovery = 91%  Analysis Date = 02/27/16 
 Pct Recovery = 91%  Analysis Date = 02/27/16 
 Pct Recovery = 91%  Analysis Date = 02/23/16 
 Pct Recovery = 92%  Analysis Date = 02/23/16 
 Pct Recovery = 92%  Analysis Date = 02/19/16 
 Pct Recovery = 92%  Analysis Date = 02/19/16 
 Pct Recovery = 92%  Analysis Date = 02/15/16 
 Pct Recovery = 92%  Analysis Date = 02/15/16 
 Pct Recovery = 92%  Analysis Date = 02/11/16 
 Pct Recovery = 93%  Analysis Date = 02/11/16 
 Pct Recovery = 93%  Analysis Date = 02/06/16 
 Pct Recovery = 93%  Analysis Date = 02/06/16 
 Pct Recovery = 93%  Analysis Date = 02/02/16 
 Pct Recovery = 93%  Analysis Date = 02/02/16 
 Pct Recovery = 93%  Analysis Date = 01/29/16 
 Pct Recovery = 93%  Analysis Date = 01/29/16 
 Pct Recovery = 93%  Analysis Date = 01/25/16 
 Pct Recovery = 93%  Analysis Date = 01/25/16 
 Pct Recovery = 93%  Analysis Date = 01/21/16 
 Pct Recovery = 93%  Analysis Date = 01/21/16 
 Pct Recovery = 93%  Analysis Date = 01/17/16 
 Pct Recovery = 93%  Analysis Date = 01/17/16 
 Pct Recovery = 93%  Analysis Date = 01/13/16 
 Pct Recovery = 94%  Analysis Date = 01/13/16 
 Pct Recovery = 94%  Analysis Date = 01/08/16 
 Pct Recovery = 94%  Analysis Date = 01/08/16 
 Pct Recovery = 94%  Analysis Date = 01/04/16 
 Pct Recovery = 94%  Analysis Date = 01/04/16 
 Pct Recovery = 94%  Analysis Date = 12/31/15 
 Pct Recovery = 94%  Analysis Date = 12/31/15 
 Pct Recovery = 94%  Analysis Date = 12/27/15 
 Pct Recovery = 94%  Analysis Date = 12/27/15 
 Pct Recovery = 94%  Analysis Date = 12/23/15 
 Pct Recovery = 94%  Analysis Date = 12/23/15 
 Pct Recovery = 94%  Analysis Date = 12/19/15 
 Pct Recovery = 95%  Analysis Date = 12/19/15 
 Pct Recovery = 95%  Analysis Date = 12/15/15 
 Pct Recovery = 95%  Analysis Date = 12/15/15 
 Pct Recovery = 95%  Analysis Date = 12/11/15 
 Pct Recovery = 95%  Analysis Date = 12/11/15 
 Pct Recovery = 95%  Analysis Date = 12/06/15 
 Pct Recovery = 95%  Analysis Date = 12/06/15 
 Pct Recovery = 95%  Analysis Date = 12/02/15 
 Pct Recovery = 95%  Analysis Date = 12/02/15 
 Pct Recovery = 95%  Analysis Date = 11/28/15 
 Pct Recovery = 95%  Analysis Date = 11/28/15 
 Pct Recovery = 95%  Analysis Date = 11/24/15 
 Pct Recovery = 95%  Analysis Date = 11/24/15 
 Pct Recovery = 95%  Analysis Date = 11/20/15 
 Pct Recovery = 95%  Analysis Date = 11/20/15 
 Pct Recovery = 95%  Analysis Date = 11/16/15 
 Pct Recovery = 95%  Analysis Date = 11/16/15 
 Pct Recovery = 95%  Analysis Date = 11/12/15 
 Pct Recovery = 95%  Analysis Date = 11/12/15 
 Pct Recovery = 95%  Analysis Date = 11/07/15 
 Pct Recovery = 95%  Analysis Date = 11/07/15 
 Pct Recovery = 95%  Analysis Date = 11/03/15 
 Pct Recovery = 95%  Analysis Date = 11/03/15 
 Pct Recovery = 95%  Analysis Date = 10/30/15 
 Pct Recovery = 95%  Analysis Date = 10/30/15 
 Pct Recovery = 95%  Analysis Date = 10/26/15 
 Pct Recovery = 95%  Analysis Date = 10/26/15 
 Pct Recovery = 95%  Analysis Date = 10/22/15 
 Pct Recovery = 95%  Analysis Date = 10/22/15 
 Pct Recovery = 95%  Analysis Date = 10/18/15 
 Pct Recovery = 95%  Analysis Date = 10/18/15 
 Pct Recovery = 95%  Analysis Date = 10/14/15 
 Pct Recovery = 95%  Analysis Date = 10/14/15 
 Pct Recovery = 95%  Analysis Date = 10/10/15 
 Pct Recovery = 96%  Analysis Date = 10/10/15 
 Pct Recovery = 96%  Analysis Date = 10/05/15 
 Pct Recovery = 96%  Analysis Date = 10/05/15 
 Pct Recovery = 96%  Analysis Date = 10/01/15 
 Pct Recovery = 96%  Analysis Date = 10/01/15 
 Pct Recovery = 96%  Analysis Date = 09/27/15 
 Pct Recovery = 96%  Analysis Date = 09/27/15 
 Pct Recovery = 96%  Analysis Date = 09/23/15 
 Pct Recovery = 96%  Analysis Date = 09/23/15 
 Pct Recovery = 96%  Analysis Date = 09/19/15 
 Pct Recovery = 97%  Analysis Date = 09/19/15 
 Pct Recovery = 97%  Analysis Date = 09/15/15 
 Pct Recovery = 97%  Analysis Date = 09/15/15 
 Pct Recovery = 97%  Analysis Date = 09/11/15 
 Pct Recovery = 97%  Analysis Date = 09/11/15 
 Pct Recovery = 97%  Analysis Date = 09/06/15 
 Pct Recovery = 97%  Analysis Date = 09/06/15 
 Pct Recovery = 97%  Analysis Date = 09/02/15 
 Pct Recovery = 97%  Analysis Date = 09/02/15 
 Pct Recovery = 97%  Analysis Date = 08/29/15 
 Pct Recovery = 98%  Analysis Date = 08/29/15 
 Pct Recovery = 98%  Analysis Date = 08/25/15 
 Pct Recovery = 98%  Analysis Date = 08/25/15 
 Pct Recovery = 98%  Analysis Date = 08/21/15 
 Pct Recovery = 98%  Analysis Date = 08/21/15 
 Pct Recovery = 98%  Analysis Date = 08/17/15 
 Pct Recovery = 98%  Analysis Date = 08/17/15 
 Pct Recovery = 98%  Analysis Date = 08/13/15 
 Pct Recovery = 99%  Analysis Date = 08/13/15 
 Pct Recovery = 99%  Analysis Date = 08/08/15 
 Pct Recovery = 99%  Analysis Date = 08/08/15 
 Pct Recovery = 99%  Analysis Date = 08/04/15 
 Pct Recovery = 99%  Analysis Date = 08/04/15 
 Pct Recovery = 99%  Analysis Date = 07/31/15 
 Pct Recovery = 100%  Analysis Date = 07/31/15 
 Pct Recovery = 100%  Analysis Date = 07/27/15 
 Pct Recovery = 100%  Analysis Date = 07/27/15 
 Pct Recovery = 100%  Analysis Date = 07/23/15 
 Pct Recovery = 100%  Analysis Date = 07/23/15 
 Pct Recovery = 100%  Analysis Date = 07/19/15 
 Pct Recovery = 100%  Analysis Date = 07/19/15 
 Pct Recovery = 100%  Analysis Date = 07/15/15 
 Pct Recovery = 101%  Analysis Date = 07/15/15 
 Pct Recovery = 101%  Analysis Date = 07/11/15 
 Pct Recovery = 101%  Analysis Date = 07/11/15 
 Pct Recovery = 101%  Analysis Date = 07/06/15 
 Pct Recovery = 101%  Analysis Date = 07/06/15 
 Pct Recovery = 101%  Analysis Date = 07/02/15 
 Pct Recovery = 102%  Analysis Date = 07/02/15 
 Pct Recovery = 102%  Analysis Date = 06/28/15 
 Pct Recovery = 102%  Analysis Date = 06/28/15 
 Pct Recovery = 102%  Analysis Date = 06/24/15 
 Pct Recovery = 102%  Analysis Date = 06/24/15 
 Pct Recovery = 102%  Analysis Date = 06/20/15 
 Pct Recovery = 102%  Analysis Date = 06/20/15 
 Pct Recovery = 102%  Analysis Date = 06/16/15 
 Pct Recovery = 103%  Analysis Date = 06/16/15 
 Pct Recovery = 103%  Analysis Date = 06/12/15 
 Pct Recovery = 103%  Analysis Date = 06/12/15 
 Pct Recovery = 103%  Analysis Date = 06/07/15 
 Pct Recovery = 103%  Analysis Date = 06/07/15 
 Pct Recovery = 103%  Analysis Date = 06/03/15 
 Pct Recovery = 104%  Analysis Date = 06/03/15 
 Pct Recovery = 104%  Analysis Date = 05/30/15 
 Pct Recovery = 104%  Analysis Date = 05/30/15 
 Pct Recovery = 104%  Analysis Date = 05/26/15 
 Pct Recovery = 104%  Analysis Date = 05/26/15 
 Pct Recovery = 104%  Analysis Date = 05/22/15 
 Pct Recovery = 105%  Analysis Date = 05/22/15 
 Pct Recovery = 105%  Analysis Date = 05/18/15 
 Pct Recovery = 105%  Analysis Date = 05/18/15 
 Pct Recovery = 105%  Analysis Date = 05/14/15 
 Pct Recovery = 105%  Analysis Date = 05/14/15 
 Pct Recovery = 105%  Analysis Date = 05/10/15 
 Pct Recovery = 106%  Analysis Date = 05/10/15 
 Pct Recovery = 106%  Analysis Date = 05/05/15 
 Pct Recovery = 106%  Analysis Date = 05/05/15 
 Pct Recovery = 106%  Analysis Date = 05/01/15 
 Pct Recovery = 106%  Analysis Date = 05/01/15 
 Pct Recovery = 106%  Analysis Date = 04/27/15 
 Pct Recovery = 106%  Analysis Date = 04/27/15 
 Pct Recovery = 106%  Analysis Date = 04/23/15 
 Pct Recovery = 106%  Analysis Date = 04/23/15 
 Pct Recovery = 106%  Analysis Date = 04/19/15 
 Pct Recovery = 106%  Analysis Date = 04/19/15 
 Pct Recovery = 106%  Analysis Date = 04/15/15 
 Pct Recovery = 107%  Analysis Date = 04/15/15 
 Pct Recovery = 107%  Analysis Date = 04/11/15 
 Pct Recovery = 107%  Analysis Date = 04/11/15 
 Pct Recovery = 107%  Analysis Date = 04/06/15 
 Pct Recovery = 107%  Analysis Date = 04/06/15 
 Pct Recovery = 107%  Analysis Date = 04/02/15 
 Pct Recovery = 107%  Analysis Date = 04/02/15 
 Pct Recovery = 107%  Analysis Date = 03/29/15 
 Pct Recovery = 107%  Analysis Date = 03/29/15 
 Pct Recovery = 107%  Analysis Date = 03/25/15 
 Pct Recovery = 107%  Analysis Date = 03/25/15 
 Pct Recovery = 107%  Analysis Date = 03/21/15 
 Pct Recovery = 107%  Analysis Date = 03/21/15 
 Pct Recovery = 107%  Analysis Date = 03/17/15 
 Pct Recovery = 108%  Analysis Date = 03/17/15 
 Pct Recovery = 108%  Analysis Date = 03/13/15 
 Pct Recovery = 108%  Analysis Date = 03/13/15 
 Pct Recovery = 108%  Analysis Date = 03/08/15 
 Pct Recovery = 108%  Analysis Date = 03/08/15 
 Pct Recovery = 108%  Analysis Date = 03/04/15 
 Pct Recovery = 108%  Analysis Date = 03/04/15 
 Pct Recovery = 108%  Analysis Date = 02/28/15 
 Pct Recovery = 108%  Analysis Date = 02/28/15 
 Pct Recovery = 108%  Analysis Date = 02/24/15 
 Pct Recovery = 108%  Analysis Date = 02/24/15 
 Pct Recovery = 108%  Analysis Date = 02/20/15 
 Pct Recovery = 109%  Analysis Date = 02/20/15 
 Pct Recovery = 109%  Analysis Date = 02/16/15 
 Pct Recovery = 109%  Analysis Date = 02/16/15 
 Pct Recovery = 109%  Analysis Date = 02/12/15 
 Pct Recovery = 109%  Analysis Date = 02/12/15 
 Pct Recovery = 109%  Analysis Date = 02/08/15 
 Pct Recovery = 109%  Analysis Date = 02/08/15 
 Pct Recovery = 109%  Analysis Date = 02/03/15 
 Pct Recovery = 109%  Analysis Date = 02/03/15 
 Pct Recovery = 109%  Analysis Date = 01/30/15 
 Pct Recovery = 109%  Analysis Date = 01/30/15 
 Pct Recovery = 109%  Analysis Date = 01/26/15 
 Pct Recovery = 110%  Analysis Date = 01/26/15 
 Pct Recovery = 110%  Analysis Date = 01/22/15 
 Pct Recovery = 110%  Analysis Date = 01/22/15 
 Pct Recovery = 110%  Analysis Date = 01/18/15 
 Pct Recovery = 110%  Analysis Date = 01/18/15 
 Pct Recovery = 110%  Analysis Date = 01/14/15 
 Pct Recovery = 110%  Analysis Date = 01/14/15 
 Pct Recovery = 110%  Analysis Date = 01/10/15 
 Pct Recovery = 110%  Analysis Date = 01/10/15 
 Pct Recovery = 110%  Analysis Date = 01/05/15 
 Pct Recovery = 110%  Analysis Date = 01/05/15 
 Pct Recovery = 110%  Analysis Date = 01/01/15 
 Pct Recovery = 110%  Analysis Date = 01/01/15 
 Pct Recovery = 110%  Analysis Date = 12/28/14 
 Pct Recovery = 110%  Analysis Date = 12/28/14 
 Pct Recovery = 110%  Analysis Date = 12/24/14 
 Pct Recovery = 110%  Analysis Date = 12/24/14 
 Pct Recovery = 110%  Analysis Date = 12/20/14 
 Pct Recovery = 110%  Analysis Date = 12/20/14 
 Pct Recovery = 110%  Analysis Date = 12/16/14 
 Pct Recovery = 110%  Analysis Date = 12/16/14 
 Pct Recovery = 110%  Analysis Date = 12/12/14 
 Pct Recovery = 110%  Analysis Date = 12/12/14 
 Pct Recovery = 110%  Analysis Date = 12/08/14 
 Pct Recovery = 110%  Analysis Date = 12/08/14 
 Pct Recovery = 110%  Analysis Date = 12/03/14 
 Pct Recovery = 110%  Analysis Date = 12/03/14 
 Pct Recovery = 110%  Analysis Date = 11/29/14 
 Pct Recovery = 110%  Analysis Date = 11/29/14 
 Pct Recovery = 110%  Analysis Date = 11/25/14 
 Pct Recovery = 110%  Analysis Date = 11/25/14 
 Pct Recovery = 110%  Analysis Date = 11/21/14 
 Pct Recovery = 110%  Analysis Date = 11/21/14 
 Pct Recovery = 110%  Analysis Date = 11/17/14 
 Pct Recovery = 110%  Analysis Date = 11/17/14 
 Pct Recovery = 110%  Analysis Date = 11/13/14 
 Pct Recovery = 110%  Analysis Date = 11/13/14 
 Pct Recovery = 110%  Analysis Date = 11/09/14 
 Pct Recovery = 110%  Analysis Date = 11/09/14 
 Pct Recovery = 110%  Analysis Date = 11/04/14 
 Pct Recovery = 110%  Analysis Date = 11/04/14 
 Pct Recovery = 110%  Analysis Date = 10/31/14 
 Pct Recovery = 110%  Analysis Date = 10/31/14 
 Pct Recovery = 110%  Analysis Date = 10/27/14 
 Pct Recovery = 110%  Analysis Date = 10/27/14 
 Pct Recovery = 110%  Analysis Date = 10/23/14 
 Pct Recovery = 110%  Analysis Date = 10/23/14 
 Pct Recovery = 110%  Analysis Date = 10/19/14 
 Pct Recovery = 110%  Analysis Date = 10/19/14 
 Pct Recovery = 110%  Analysis Date = 10/15/14 
 Pct Recovery = 110%  Analysis Date = 10/15/14 
 Pct Recovery = 110%  Analysis Date = 10/11/14 
 Pct Recovery = 110%  Analysis Date = 10/11/14 
 Pct Recovery = 110%  Analysis Date = 10/06/14 
 Pct Recovery = 110%  Analysis Date = 10/06/14 
 Pct Recovery = 110%  Analysis Date = 10/02/14 
 Pct Recovery = 110%  Analysis Date = 10/02/14 
 Pct Recovery = 110%  Analysis Date = 09/28/14 
 Pct Recovery = 110%  Analysis Date = 09/28/14 
 Pct Recovery = 110%  Analysis Date = 09/24/14 
 Pct Recovery = 110%  Analysis Date = 09/24/14 
 Pct Recovery = 110%  Analysis Date = 09/20/14 
 Pct Recovery = 110%  Analysis Date = 09/20/14 
 Pct Recovery = 110%  Analysis Date = 09/16/14 
 Pct Recovery = 110%  Analysis Date = 09/16/14 
 Pct Recovery = 110%  Analysis Date = 09/12/14 
 Pct Recovery = 110%  Analysis Date = 09/12/14 
 Pct Recovery = 110%  Analysis Date = 09/08/14 
 Pct Recovery = 110%  Analysis Date = 09/08/14 
 Pct Recovery = 110%  Analysis Date = 09/03/14 
 Pct Recovery = 110%  Analysis Date = 09/03/14 
 Pct Recovery = 110%  Analysis Date = 08/30/14 
 Pct Recovery = 110%  Analysis Date = 08/30/14 
 Pct Recovery = 110%  Analysis Date = 08/26/14 
 Pct Recovery = 110%  Analysis Date = 08/26/14 
 Pct Recovery = 110%  Analysis Date = 08/22/14 
 Pct Recovery = 110%  Analysis Date = 08/22/14 
 Pct Recovery = 110%  Analysis Date = 08/18/14 
 Pct Recovery = 110%  Analysis Date = 08/18/14 
 Pct Recovery = 110%  Analysis Date = 08/14/14 
 Pct Recovery = 110%  Analysis Date = 08/14/14 
 Pct Recovery = 110%  Analysis Date = 08/10/14 
 Pct Recovery = 110%  Analysis Date = 08/10/14 
 Pct Recovery = 110%  Analysis Date = 08/05/14 
 Pct Recovery = 110%  Analysis Date = 08/05/14 
 Pct Recovery = 110%  Analysis Date = 08/01/14 
 Pct Recovery = 110%  Analysis Date = 08/01/14 
 Pct Recovery = 110%  Analysis Date = 07/28/14 
 Pct Recovery = 110%  Analysis Date = 07/28/14 
 Pct Recovery = 110%  Analysis Date = 07/24/14 
 Pct Recovery = 110%  Analysis Date = 07/24/14 
 Pct Recovery = 110%  Analysis Date = 07/20/14 
 Pct Recovery = 110%  Analysis Date = 07/20/14 
 Pct Recovery = 110%  Analysis Date = 07/16/14 
 Pct Recovery = 110%  Analysis Date = 07/16/14 
 Pct Recovery = 110%  Analysis Date = 07/12/14 
 Pct Recovery = 110%  Analysis Date = 07/12/14 
 Pct Recovery = 110%  Analysis Date = 07/08/14 
 Pct Recovery = 110%  Analysis Date = 07/08/14 
 Pct Recovery = 110%  Analysis Date = 07/03/14 
 Pct Recovery = 110%  Analysis Date = 07/03/14 
 Pct Recovery = 110%  Analysis Date = 06/29/14 
 Pct Recovery = 110%  Analysis Date = 06/29/14 
 Pct Recovery = 110%  Analysis Date = 06/25/14 
 Pct Recovery = 110%  Analysis Date = 06/25/14 
 Pct Recovery = 110%  Analysis Date = 06/21/14 
 Pct Recovery = 110%  Analysis Date = 06/21/14 
 Pct Recovery = 110%  Analysis Date = 06/17/14 
 Pct Recovery = 110%  Analysis Date = 06/17/14 
 Pct Recovery = 110%  Analysis Date = 06/13/14 
 Pct Recovery = 110%  Analysis Date = 06/13/14 
 Pct Recovery = 110%  Analysis Date = 06/09/14 
 Pct Recovery = 110%  Analysis Date = 06/09/14 
 Pct Recovery = 110%  Analysis Date = 06/04/14 
 Pct Recovery = 110%  Analysis Date = 06/04/14 
 Pct Recovery = 110%  Analysis Date = 05/31/14 
 Pct Recovery = 110%  Analysis Date = 05/31/14 
 Pct Recovery = 110%  Analysis Date = 05/27/14 
 Pct Recovery = 110%  Analysis Date = 05/27/14 
 Pct Recovery = 110%  Analysis Date = 05/23/14 
 Pct Recovery = 110%  Analysis Date = 05/23/14 
 Pct Recovery = 110%  Analysis Date = 05/19/14 
 Pct Recovery = 110%  Analysis Date = 05/19/14 
 Pct Recovery = 110%  Analysis Date = 05/15/14 
 Pct Recovery = 110%  Analysis Date = 05/15/14 
 Pct Recovery = 110%  Analysis Date = 05/11/14 
 Pct Recovery = 110%  Analysis Date = 05/11/14 
 Pct Recovery = 110%  Analysis Date = 05/07/14 
 Pct Recovery = 110%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
ACETATE, ISOPROPYL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 38 98% 15% 98% 17%
Total 38 98% 15% 98% 17%

Sample Statistics
ACETATE, ISOPROPYL

Characteristic N % % Basis
Plotted 38 100% Spiked
Estimated Values 1 3% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 38 .  
False Negatives 0 0% 0 out of 38
Not Spiked 17 .  
False Positives 1 6% 1 out of 17

BQS OBSP Determination:
ACETATE, PROPYL
METHOD: 4437 , TESTIDCODE: 45022GM016
Open Data Set

 Analysis Date = 07/29/16 
 SpikeMix = Supelco LC20145V: 40 µl & NSI 041516: 40 µl & NSI 041416HVOC: 40 µl 
 Pct Recovery = 85%  Analysis Date = 07/06/16 
 SpikeMix = Accu 216041354: 40 µl & NSI 041516: 40 µl & NSI 041416HVOC: 40 µl 
 Pct Recovery = 71%  Analysis Date = 08/11/16 
 SpikeMix = Phenova B20160303: 25 µl & Supelco LC20145V: 25 µl & NSI 041416HVOC: 25 µl 
 Pct Recovery = 85%  Analysis Date = 07/14/16 
 SpikeMix = NSI 041516: 25 µl & ChemService 5082800: 25 µl & NSI 041416HVOC: 25 µl 
 Pct Recovery = 84%  Analysis Date = 05/21/16 
 SpikeMix = Supelco LC20145V: 25 µl & NSI 041516: 25 µl & NSI 041416HVOC: 25 µl 
 Pct Recovery = 102%  Analysis Date = 03/19/15 
 SpikeMix = Supelco LC06437: 20 µl & NSI 031814: 20 µl 
 Pct Recovery = 180%  Analysis Date = 01/10/15 
 SpikeMix = Abs 032014: 20 µl & ERA 0321-14-05A: 20 µl 
 Pct Recovery = 150%  Analysis Date = 08/20/14 
 SpikeMix = Supelco LC06437: 20 µl & Abs 032014: 20 µl 
 Pct Recovery = 123%  Analysis Date = 07/23/14 
 SpikeMix = Accu 214031128: 20 µl & Abs 032014: 20 µl 
 Pct Recovery = 130%  Analysis Date = 07/03/14 
 SpikeMix = Abs 032014: 20 µl & ChemService 2615700: 20 µl 
 Pct Recovery = 145%  Analysis Date = 06/06/14 
 SpikeMix = NSI 031814: 20 µl & ChemService 2615700: 20 µl 
 Pct Recovery = 120%  Analysis Date = 05/07/14 
 SpikeMix = NSI 031814: 20 µl & Accu 214031128: 20 µl 
 Pct Recovery = 93%  Analysis Date = 01/22/16 
 SpikeMix = NSI 050515HVOC: 25 µl & ERA 0601-15-05: 25 µl 
 Pct Recovery = 98%  Analysis Date = 10/09/15 
 SpikeMix = ERA 0601-15-05: 25 µl & Accu 215041338: 25 µl 
 Pct Recovery = 100%  Analysis Date = 06/26/15 
 SpikeMix = ChemService 3818700: 25 µl & Accu 215041338: 25 µl 
 Pct Recovery = 99%  Analysis Date = 06/25/15 
 SpikeMix = ChemService 3818700: 25 µl & NSI 050515HVOC: 25 µl 
 Pct Recovery = 91%  Analysis Date = 07/06/16 
 SpikeMix = Phenova B20160303: 15 µl & Accu 216041354: 15 µl & NSI 041416HVOC: 15 µl 
 Pct Recovery = 85%  Analysis Date = 06/03/16 
 SpikeMix = NSI 041516: 15 µl & Phenova B20160303: 15 µl & NSI 041416HVOC: 15 µl 
 Pct Recovery = 94%  Analysis Date = 07/27/16 
 SpikeMix = ChemService 5082800: 15 µl & Supelco LC20145V: 15 µl & Accu 216041225: 15 µl 
 Pct Recovery = 94%  Analysis Date = 05/20/16 
 SpikeMix = Accu 216041354: 15 µl & NSI 041516: 15 µl & Accu 216041225: 15 µl 
 Pct Recovery = 116%  Analysis Date = 09/24/15 
 SpikeMix = Abs 040315: 15 µl & ERA 0601-15-05: 15 µl 
 Pct Recovery = 93%  Analysis Date = 08/24/15 
 SpikeMix = ERA 0601-15-05: 15 µl & Supelco LC13544: 15 µl 
 Pct Recovery = 75%  Analysis Date = 04/28/16 
 SpikeMix = ChemService 3818700: 15 µl & Supelco LC13544: 15 µl 
 Pct Recovery = 112%  Analysis Date = 06/16/15 
 SpikeMix = ChemService 3818700: 15 µl & NSI 050515HVOC: 15 µl 
 Pct Recovery = 88%  Analysis Date = 05/14/15 
 SpikeMix = ChemService 3818700: 15 µl & Supelco LC13544: 15 µl 
 Pct Recovery = 107%  Analysis Date = 04/25/15 
 SpikeMix = Abs 032014: 10 µl & ERA 0321-14-05A: 10 µl 
 Pct Recovery = 115%  Analysis Date = 12/13/14 
 SpikeMix = Accu 214031128: 10 µl & NSI 031814: 10 µl 
 Pct Recovery = 113%  Analysis Date = 09/11/14 
 SpikeMix = Accu 214031128: 10 µl & Abs 032014: 10 µl 
 Pct Recovery = 135%  Analysis Date = 07/30/14 
 SpikeMix = NSI 031814: 10 µl & ChemService 2615700: 10 µl 
 Pct Recovery = 131%  Analysis Date = 06/17/14 
 SpikeMix = Supelco LC06437: 10 µl & Abs 032014: 10 µl 
 Pct Recovery = 148%  Analysis Date = 02/12/16 
 SpikeMix = ERA 0601-15-05: 10 µl & Accu 215041338: 10 µl 
 Pct Recovery = 91%  Analysis Date = 12/05/15 
 SpikeMix = NSI 050515HVOC: 10 µl & ERA 0601-15-05: 10 µl 
 Pct Recovery = 96%  Analysis Date = 11/14/15 
 SpikeMix = ERA 0601-15-05: 10 µl 
 Pct Recovery = 93%  Analysis Date = 08/14/15 
 SpikeMix = Abs 040315: 10 µl & ERA 0601-15-05: 10 µl 
 Pct Recovery = 93%  Analysis Date = 04/09/16 
 SpikeMix = Abs 040315: 10 µl & ChemService 3818700: 10 µl 
 Pct Recovery = 127%  Analysis Date = 12/10/15 
 SpikeMix = ChemService 3818700: 10 µl & Supelco LC13544: 10 µl 
 Pct Recovery = 112%  Analysis Date = 10/23/15 
 SpikeMix = Abs 040315: 10 µl & ChemService 3818700: 10 µl 
 Pct Recovery = 148%  Analysis Date = 05/20/15 
 SpikeMix = ChemService 3818700: 10 µl & Accu 215041338: 10 µl 
 Pct Recovery = 115%  Analysis Date = 08/10/16 
 Pct Recovery = 89%  Analysis Date = 08/06/16 
 Pct Recovery = 90%  Analysis Date = 08/06/16 
 Pct Recovery = 90%  Analysis Date = 08/02/16 
 Pct Recovery = 90%  Analysis Date = 08/02/16 
 Pct Recovery = 90%  Analysis Date = 07/29/16 
 Pct Recovery = 90%  Analysis Date = 07/29/16 
 Pct Recovery = 90%  Analysis Date = 07/25/16 
 Pct Recovery = 91%  Analysis Date = 07/25/16 
 Pct Recovery = 91%  Analysis Date = 07/21/16 
 Pct Recovery = 91%  Analysis Date = 07/21/16 
 Pct Recovery = 91%  Analysis Date = 07/17/16 
 Pct Recovery = 91%  Analysis Date = 07/17/16 
 Pct Recovery = 91%  Analysis Date = 07/13/16 
 Pct Recovery = 92%  Analysis Date = 07/13/16 
 Pct Recovery = 92%  Analysis Date = 07/08/16 
 Pct Recovery = 92%  Analysis Date = 07/08/16 
 Pct Recovery = 92%  Analysis Date = 07/04/16 
 Pct Recovery = 92%  Analysis Date = 07/04/16 
 Pct Recovery = 92%  Analysis Date = 06/30/16 
 Pct Recovery = 93%  Analysis Date = 06/30/16 
 Pct Recovery = 93%  Analysis Date = 06/26/16 
 Pct Recovery = 93%  Analysis Date = 06/26/16 
 Pct Recovery = 93%  Analysis Date = 06/22/16 
 Pct Recovery = 93%  Analysis Date = 06/22/16 
 Pct Recovery = 93%  Analysis Date = 06/18/16 
 Pct Recovery = 94%  Analysis Date = 06/18/16 
 Pct Recovery = 94%  Analysis Date = 06/14/16 
 Pct Recovery = 94%  Analysis Date = 06/14/16 
 Pct Recovery = 94%  Analysis Date = 06/09/16 
 Pct Recovery = 94%  Analysis Date = 06/09/16 
 Pct Recovery = 94%  Analysis Date = 06/05/16 
 Pct Recovery = 95%  Analysis Date = 06/05/16 
 Pct Recovery = 95%  Analysis Date = 06/01/16 
 Pct Recovery = 95%  Analysis Date = 06/01/16 
 Pct Recovery = 95%  Analysis Date = 05/28/16 
 Pct Recovery = 95%  Analysis Date = 05/28/16 
 Pct Recovery = 95%  Analysis Date = 05/24/16 
 Pct Recovery = 95%  Analysis Date = 05/24/16 
 Pct Recovery = 95%  Analysis Date = 05/20/16 
 Pct Recovery = 96%  Analysis Date = 05/20/16 
 Pct Recovery = 96%  Analysis Date = 05/16/16 
 Pct Recovery = 96%  Analysis Date = 05/16/16 
 Pct Recovery = 96%  Analysis Date = 05/12/16 
 Pct Recovery = 96%  Analysis Date = 05/12/16 
 Pct Recovery = 96%  Analysis Date = 05/07/16 
 Pct Recovery = 97%  Analysis Date = 05/07/16 
 Pct Recovery = 97%  Analysis Date = 05/03/16 
 Pct Recovery = 97%  Analysis Date = 05/03/16 
 Pct Recovery = 97%  Analysis Date = 04/29/16 
 Pct Recovery = 97%  Analysis Date = 04/29/16 
 Pct Recovery = 97%  Analysis Date = 04/25/16 
 Pct Recovery = 97%  Analysis Date = 04/25/16 
 Pct Recovery = 97%  Analysis Date = 04/21/16 
 Pct Recovery = 98%  Analysis Date = 04/21/16 
 Pct Recovery = 98%  Analysis Date = 04/17/16 
 Pct Recovery = 98%  Analysis Date = 04/17/16 
 Pct Recovery = 98%  Analysis Date = 04/13/16 
 Pct Recovery = 98%  Analysis Date = 04/13/16 
 Pct Recovery = 98%  Analysis Date = 04/08/16 
 Pct Recovery = 99%  Analysis Date = 04/08/16 
 Pct Recovery = 99%  Analysis Date = 04/04/16 
 Pct Recovery = 99%  Analysis Date = 04/04/16 
 Pct Recovery = 99%  Analysis Date = 03/31/16 
 Pct Recovery = 99%  Analysis Date = 03/31/16 
 Pct Recovery = 99%  Analysis Date = 03/27/16 
 Pct Recovery = 100%  Analysis Date = 03/27/16 
 Pct Recovery = 100%  Analysis Date = 03/23/16 
 Pct Recovery = 100%  Analysis Date = 03/23/16 
 Pct Recovery = 100%  Analysis Date = 03/19/16 
 Pct Recovery = 100%  Analysis Date = 03/19/16 
 Pct Recovery = 100%  Analysis Date = 03/15/16 
 Pct Recovery = 100%  Analysis Date = 03/15/16 
 Pct Recovery = 100%  Analysis Date = 03/11/16 
 Pct Recovery = 101%  Analysis Date = 03/11/16 
 Pct Recovery = 101%  Analysis Date = 03/06/16 
 Pct Recovery = 101%  Analysis Date = 03/06/16 
 Pct Recovery = 101%  Analysis Date = 03/02/16 
 Pct Recovery = 101%  Analysis Date = 03/02/16 
 Pct Recovery = 101%  Analysis Date = 02/27/16 
 Pct Recovery = 102%  Analysis Date = 02/27/16 
 Pct Recovery = 102%  Analysis Date = 02/23/16 
 Pct Recovery = 102%  Analysis Date = 02/23/16 
 Pct Recovery = 102%  Analysis Date = 02/19/16 
 Pct Recovery = 102%  Analysis Date = 02/19/16 
 Pct Recovery = 102%  Analysis Date = 02/15/16 
 Pct Recovery = 103%  Analysis Date = 02/15/16 
 Pct Recovery = 103%  Analysis Date = 02/11/16 
 Pct Recovery = 103%  Analysis Date = 02/11/16 
 Pct Recovery = 103%  Analysis Date = 02/06/16 
 Pct Recovery = 103%  Analysis Date = 02/06/16 
 Pct Recovery = 103%  Analysis Date = 02/02/16 
 Pct Recovery = 103%  Analysis Date = 02/02/16 
 Pct Recovery = 103%  Analysis Date = 01/29/16 
 Pct Recovery = 103%  Analysis Date = 01/29/16 
 Pct Recovery = 103%  Analysis Date = 01/25/16 
 Pct Recovery = 103%  Analysis Date = 01/25/16 
 Pct Recovery = 103%  Analysis Date = 01/21/16 
 Pct Recovery = 103%  Analysis Date = 01/21/16 
 Pct Recovery = 103%  Analysis Date = 01/17/16 
 Pct Recovery = 103%  Analysis Date = 01/17/16 
 Pct Recovery = 103%  Analysis Date = 01/13/16 
 Pct Recovery = 103%  Analysis Date = 01/13/16 
 Pct Recovery = 103%  Analysis Date = 01/08/16 
 Pct Recovery = 103%  Analysis Date = 01/08/16 
 Pct Recovery = 103%  Analysis Date = 01/04/16 
 Pct Recovery = 103%  Analysis Date = 01/04/16 
 Pct Recovery = 103%  Analysis Date = 12/31/15 
 Pct Recovery = 103%  Analysis Date = 12/31/15 
 Pct Recovery = 103%  Analysis Date = 12/27/15 
 Pct Recovery = 103%  Analysis Date = 12/27/15 
 Pct Recovery = 103%  Analysis Date = 12/23/15 
 Pct Recovery = 103%  Analysis Date = 12/23/15 
 Pct Recovery = 103%  Analysis Date = 12/19/15 
 Pct Recovery = 103%  Analysis Date = 12/19/15 
 Pct Recovery = 103%  Analysis Date = 12/15/15 
 Pct Recovery = 103%  Analysis Date = 12/15/15 
 Pct Recovery = 103%  Analysis Date = 12/11/15 
 Pct Recovery = 103%  Analysis Date = 12/11/15 
 Pct Recovery = 103%  Analysis Date = 12/06/15 
 Pct Recovery = 103%  Analysis Date = 12/06/15 
 Pct Recovery = 103%  Analysis Date = 12/02/15 
 Pct Recovery = 103%  Analysis Date = 12/02/15 
 Pct Recovery = 103%  Analysis Date = 11/28/15 
 Pct Recovery = 103%  Analysis Date = 11/28/15 
 Pct Recovery = 103%  Analysis Date = 11/24/15 
 Pct Recovery = 103%  Analysis Date = 11/24/15 
 Pct Recovery = 103%  Analysis Date = 11/20/15 
 Pct Recovery = 102%  Analysis Date = 11/20/15 
 Pct Recovery = 102%  Analysis Date = 11/16/15 
 Pct Recovery = 102%  Analysis Date = 11/16/15 
 Pct Recovery = 102%  Analysis Date = 11/12/15 
 Pct Recovery = 102%  Analysis Date = 11/12/15 
 Pct Recovery = 102%  Analysis Date = 11/07/15 
 Pct Recovery = 102%  Analysis Date = 11/07/15 
 Pct Recovery = 102%  Analysis Date = 11/03/15 
 Pct Recovery = 102%  Analysis Date = 11/03/15 
 Pct Recovery = 102%  Analysis Date = 10/30/15 
 Pct Recovery = 101%  Analysis Date = 10/30/15 
 Pct Recovery = 101%  Analysis Date = 10/26/15 
 Pct Recovery = 101%  Analysis Date = 10/26/15 
 Pct Recovery = 101%  Analysis Date = 10/22/15 
 Pct Recovery = 101%  Analysis Date = 10/22/15 
 Pct Recovery = 101%  Analysis Date = 10/18/15 
 Pct Recovery = 101%  Analysis Date = 10/18/15 
 Pct Recovery = 101%  Analysis Date = 10/14/15 
 Pct Recovery = 102%  Analysis Date = 10/14/15 
 Pct Recovery = 102%  Analysis Date = 10/10/15 
 Pct Recovery = 102%  Analysis Date = 10/10/15 
 Pct Recovery = 102%  Analysis Date = 10/05/15 
 Pct Recovery = 102%  Analysis Date = 10/05/15 
 Pct Recovery = 102%  Analysis Date = 10/01/15 
 Pct Recovery = 102%  Analysis Date = 10/01/15 
 Pct Recovery = 102%  Analysis Date = 09/27/15 
 Pct Recovery = 102%  Analysis Date = 09/27/15 
 Pct Recovery = 102%  Analysis Date = 09/23/15 
 Pct Recovery = 103%  Analysis Date = 09/23/15 
 Pct Recovery = 103%  Analysis Date = 09/19/15 
 Pct Recovery = 103%  Analysis Date = 09/19/15 
 Pct Recovery = 103%  Analysis Date = 09/15/15 
 Pct Recovery = 103%  Analysis Date = 09/15/15 
 Pct Recovery = 103%  Analysis Date = 09/11/15 
 Pct Recovery = 103%  Analysis Date = 09/11/15 
 Pct Recovery = 103%  Analysis Date = 09/06/15 
 Pct Recovery = 103%  Analysis Date = 09/06/15 
 Pct Recovery = 103%  Analysis Date = 09/02/15 
 Pct Recovery = 104%  Analysis Date = 09/02/15 
 Pct Recovery = 104%  Analysis Date = 08/29/15 
 Pct Recovery = 104%  Analysis Date = 08/29/15 
 Pct Recovery = 104%  Analysis Date = 08/25/15 
 Pct Recovery = 104%  Analysis Date = 08/25/15 
 Pct Recovery = 104%  Analysis Date = 08/21/15 
 Pct Recovery = 104%  Analysis Date = 08/21/15 
 Pct Recovery = 104%  Analysis Date = 08/17/15 
 Pct Recovery = 105%  Analysis Date = 08/17/15 
 Pct Recovery = 105%  Analysis Date = 08/13/15 
 Pct Recovery = 105%  Analysis Date = 08/13/15 
 Pct Recovery = 105%  Analysis Date = 08/08/15 
 Pct Recovery = 106%  Analysis Date = 08/08/15 
 Pct Recovery = 106%  Analysis Date = 08/04/15 
 Pct Recovery = 106%  Analysis Date = 08/04/15 
 Pct Recovery = 106%  Analysis Date = 07/31/15 
 Pct Recovery = 107%  Analysis Date = 07/31/15 
 Pct Recovery = 107%  Analysis Date = 07/27/15 
 Pct Recovery = 107%  Analysis Date = 07/27/15 
 Pct Recovery = 107%  Analysis Date = 07/23/15 
 Pct Recovery = 108%  Analysis Date = 07/23/15 
 Pct Recovery = 108%  Analysis Date = 07/19/15 
 Pct Recovery = 108%  Analysis Date = 07/19/15 
 Pct Recovery = 108%  Analysis Date = 07/15/15 
 Pct Recovery = 109%  Analysis Date = 07/15/15 
 Pct Recovery = 109%  Analysis Date = 07/11/15 
 Pct Recovery = 109%  Analysis Date = 07/11/15 
 Pct Recovery = 109%  Analysis Date = 07/06/15 
 Pct Recovery = 110%  Analysis Date = 07/06/15 
 Pct Recovery = 110%  Analysis Date = 07/02/15 
 Pct Recovery = 110%  Analysis Date = 07/02/15 
 Pct Recovery = 110%  Analysis Date = 06/28/15 
 Pct Recovery = 110%  Analysis Date = 06/28/15 
 Pct Recovery = 110%  Analysis Date = 06/24/15 
 Pct Recovery = 111%  Analysis Date = 06/24/15 
 Pct Recovery = 111%  Analysis Date = 06/20/15 
 Pct Recovery = 111%  Analysis Date = 06/20/15 
 Pct Recovery = 111%  Analysis Date = 06/16/15 
 Pct Recovery = 112%  Analysis Date = 06/16/15 
 Pct Recovery = 112%  Analysis Date = 06/12/15 
 Pct Recovery = 112%  Analysis Date = 06/12/15 
 Pct Recovery = 112%  Analysis Date = 06/07/15 
 Pct Recovery = 113%  Analysis Date = 06/07/15 
 Pct Recovery = 113%  Analysis Date = 06/03/15 
 Pct Recovery = 113%  Analysis Date = 06/03/15 
 Pct Recovery = 113%  Analysis Date = 05/30/15 
 Pct Recovery = 114%  Analysis Date = 05/30/15 
 Pct Recovery = 114%  Analysis Date = 05/26/15 
 Pct Recovery = 114%  Analysis Date = 05/26/15 
 Pct Recovery = 114%  Analysis Date = 05/22/15 
 Pct Recovery = 115%  Analysis Date = 05/22/15 
 Pct Recovery = 115%  Analysis Date = 05/18/15 
 Pct Recovery = 115%  Analysis Date = 05/18/15 
 Pct Recovery = 115%  Analysis Date = 05/14/15 
 Pct Recovery = 116%  Analysis Date = 05/14/15 
 Pct Recovery = 116%  Analysis Date = 05/10/15 
 Pct Recovery = 116%  Analysis Date = 05/10/15 
 Pct Recovery = 116%  Analysis Date = 05/05/15 
 Pct Recovery = 116%  Analysis Date = 05/05/15 
 Pct Recovery = 116%  Analysis Date = 05/01/15 
 Pct Recovery = 117%  Analysis Date = 05/01/15 
 Pct Recovery = 117%  Analysis Date = 04/27/15 
 Pct Recovery = 117%  Analysis Date = 04/27/15 
 Pct Recovery = 117%  Analysis Date = 04/23/15 
 Pct Recovery = 117%  Analysis Date = 04/23/15 
 Pct Recovery = 117%  Analysis Date = 04/19/15 
 Pct Recovery = 117%  Analysis Date = 04/19/15 
 Pct Recovery = 117%  Analysis Date = 04/15/15 
 Pct Recovery = 118%  Analysis Date = 04/15/15 
 Pct Recovery = 118%  Analysis Date = 04/11/15 
 Pct Recovery = 118%  Analysis Date = 04/11/15 
 Pct Recovery = 118%  Analysis Date = 04/06/15 
 Pct Recovery = 118%  Analysis Date = 04/06/15 
 Pct Recovery = 118%  Analysis Date = 04/02/15 
 Pct Recovery = 119%  Analysis Date = 04/02/15 
 Pct Recovery = 119%  Analysis Date = 03/29/15 
 Pct Recovery = 119%  Analysis Date = 03/29/15 
 Pct Recovery = 119%  Analysis Date = 03/25/15 
 Pct Recovery = 119%  Analysis Date = 03/25/15 
 Pct Recovery = 119%  Analysis Date = 03/21/15 
 Pct Recovery = 120%  Analysis Date = 03/21/15 
 Pct Recovery = 120%  Analysis Date = 03/17/15 
 Pct Recovery = 120%  Analysis Date = 03/17/15 
 Pct Recovery = 120%  Analysis Date = 03/13/15 
 Pct Recovery = 120%  Analysis Date = 03/13/15 
 Pct Recovery = 120%  Analysis Date = 03/08/15 
 Pct Recovery = 121%  Analysis Date = 03/08/15 
 Pct Recovery = 121%  Analysis Date = 03/04/15 
 Pct Recovery = 121%  Analysis Date = 03/04/15 
 Pct Recovery = 121%  Analysis Date = 02/28/15 
 Pct Recovery = 121%  Analysis Date = 02/28/15 
 Pct Recovery = 121%  Analysis Date = 02/24/15 
 Pct Recovery = 122%  Analysis Date = 02/24/15 
 Pct Recovery = 122%  Analysis Date = 02/20/15 
 Pct Recovery = 122%  Analysis Date = 02/20/15 
 Pct Recovery = 122%  Analysis Date = 02/16/15 
 Pct Recovery = 122%  Analysis Date = 02/16/15 
 Pct Recovery = 122%  Analysis Date = 02/12/15 
 Pct Recovery = 123%  Analysis Date = 02/12/15 
 Pct Recovery = 123%  Analysis Date = 02/08/15 
 Pct Recovery = 123%  Analysis Date = 02/08/15 
 Pct Recovery = 123%  Analysis Date = 02/03/15 
 Pct Recovery = 123%  Analysis Date = 02/03/15 
 Pct Recovery = 123%  Analysis Date = 01/30/15 
 Pct Recovery = 124%  Analysis Date = 01/30/15 
 Pct Recovery = 124%  Analysis Date = 01/26/15 
 Pct Recovery = 124%  Analysis Date = 01/26/15 
 Pct Recovery = 124%  Analysis Date = 01/22/15 
 Pct Recovery = 124%  Analysis Date = 01/22/15 
 Pct Recovery = 124%  Analysis Date = 01/18/15 
 Pct Recovery = 125%  Analysis Date = 01/18/15 
 Pct Recovery = 125%  Analysis Date = 01/14/15 
 Pct Recovery = 125%  Analysis Date = 01/14/15 
 Pct Recovery = 125%  Analysis Date = 01/10/15 
 Pct Recovery = 125%  Analysis Date = 01/10/15 
 Pct Recovery = 125%  Analysis Date = 01/05/15 
 Pct Recovery = 125%  Analysis Date = 01/05/15 
 Pct Recovery = 125%  Analysis Date = 01/01/15 
 Pct Recovery = 126%  Analysis Date = 01/01/15 
 Pct Recovery = 126%  Analysis Date = 12/28/14 
 Pct Recovery = 126%  Analysis Date = 12/28/14 
 Pct Recovery = 126%  Analysis Date = 12/24/14 
 Pct Recovery = 126%  Analysis Date = 12/24/14 
 Pct Recovery = 126%  Analysis Date = 12/20/14 
 Pct Recovery = 126%  Analysis Date = 12/20/14 
 Pct Recovery = 126%  Analysis Date = 12/16/14 
 Pct Recovery = 126%  Analysis Date = 12/16/14 
 Pct Recovery = 126%  Analysis Date = 12/12/14 
 Pct Recovery = 126%  Analysis Date = 12/12/14 
 Pct Recovery = 126%  Analysis Date = 12/08/14 
 Pct Recovery = 126%  Analysis Date = 12/08/14 
 Pct Recovery = 126%  Analysis Date = 12/03/14 
 Pct Recovery = 126%  Analysis Date = 12/03/14 
 Pct Recovery = 126%  Analysis Date = 11/29/14 
 Pct Recovery = 126%  Analysis Date = 11/29/14 
 Pct Recovery = 126%  Analysis Date = 11/25/14 
 Pct Recovery = 126%  Analysis Date = 11/25/14 
 Pct Recovery = 126%  Analysis Date = 11/21/14 
 Pct Recovery = 126%  Analysis Date = 11/21/14 
 Pct Recovery = 126%  Analysis Date = 11/17/14 
 Pct Recovery = 126%  Analysis Date = 11/17/14 
 Pct Recovery = 126%  Analysis Date = 11/13/14 
 Pct Recovery = 127%  Analysis Date = 11/13/14 
 Pct Recovery = 127%  Analysis Date = 11/09/14 
 Pct Recovery = 127%  Analysis Date = 11/09/14 
 Pct Recovery = 127%  Analysis Date = 11/04/14 
 Pct Recovery = 127%  Analysis Date = 11/04/14 
 Pct Recovery = 127%  Analysis Date = 10/31/14 
 Pct Recovery = 127%  Analysis Date = 10/31/14 
 Pct Recovery = 127%  Analysis Date = 10/27/14 
 Pct Recovery = 127%  Analysis Date = 10/27/14 
 Pct Recovery = 127%  Analysis Date = 10/23/14 
 Pct Recovery = 127%  Analysis Date = 10/23/14 
 Pct Recovery = 127%  Analysis Date = 10/19/14 
 Pct Recovery = 127%  Analysis Date = 10/19/14 
 Pct Recovery = 127%  Analysis Date = 10/15/14 
 Pct Recovery = 127%  Analysis Date = 10/15/14 
 Pct Recovery = 127%  Analysis Date = 10/11/14 
 Pct Recovery = 127%  Analysis Date = 10/11/14 
 Pct Recovery = 127%  Analysis Date = 10/06/14 
 Pct Recovery = 127%  Analysis Date = 10/06/14 
 Pct Recovery = 127%  Analysis Date = 10/02/14 
 Pct Recovery = 127%  Analysis Date = 10/02/14 
 Pct Recovery = 127%  Analysis Date = 09/28/14 
 Pct Recovery = 128%  Analysis Date = 09/28/14 
 Pct Recovery = 128%  Analysis Date = 09/24/14 
 Pct Recovery = 128%  Analysis Date = 09/24/14 
 Pct Recovery = 128%  Analysis Date = 09/20/14 
 Pct Recovery = 128%  Analysis Date = 09/20/14 
 Pct Recovery = 128%  Analysis Date = 09/16/14 
 Pct Recovery = 128%  Analysis Date = 09/16/14 
 Pct Recovery = 128%  Analysis Date = 09/12/14 
 Pct Recovery = 128%  Analysis Date = 09/12/14 
 Pct Recovery = 128%  Analysis Date = 09/08/14 
 Pct Recovery = 128%  Analysis Date = 09/08/14 
 Pct Recovery = 128%  Analysis Date = 09/03/14 
 Pct Recovery = 128%  Analysis Date = 09/03/14 
 Pct Recovery = 128%  Analysis Date = 08/30/14 
 Pct Recovery = 128%  Analysis Date = 08/30/14 
 Pct Recovery = 128%  Analysis Date = 08/26/14 
 Pct Recovery = 128%  Analysis Date = 08/26/14 
 Pct Recovery = 128%  Analysis Date = 08/22/14 
 Pct Recovery = 128%  Analysis Date = 08/22/14 
 Pct Recovery = 128%  Analysis Date = 08/18/14 
 Pct Recovery = 128%  Analysis Date = 08/18/14 
 Pct Recovery = 128%  Analysis Date = 08/14/14 
 Pct Recovery = 128%  Analysis Date = 08/14/14 
 Pct Recovery = 128%  Analysis Date = 08/10/14 
 Pct Recovery = 128%  Analysis Date = 08/10/14 
 Pct Recovery = 128%  Analysis Date = 08/05/14 
 Pct Recovery = 128%  Analysis Date = 08/05/14 
 Pct Recovery = 128%  Analysis Date = 08/01/14 
 Pct Recovery = 128%  Analysis Date = 08/01/14 
 Pct Recovery = 128%  Analysis Date = 07/28/14 
 Pct Recovery = 128%  Analysis Date = 07/28/14 
 Pct Recovery = 128%  Analysis Date = 07/24/14 
 Pct Recovery = 128%  Analysis Date = 07/24/14 
 Pct Recovery = 128%  Analysis Date = 07/20/14 
 Pct Recovery = 128%  Analysis Date = 07/20/14 
 Pct Recovery = 128%  Analysis Date = 07/16/14 
 Pct Recovery = 129%  Analysis Date = 07/16/14 
 Pct Recovery = 129%  Analysis Date = 07/12/14 
 Pct Recovery = 129%  Analysis Date = 07/12/14 
 Pct Recovery = 129%  Analysis Date = 07/08/14 
 Pct Recovery = 129%  Analysis Date = 07/08/14 
 Pct Recovery = 129%  Analysis Date = 07/03/14 
 Pct Recovery = 129%  Analysis Date = 07/03/14 
 Pct Recovery = 129%  Analysis Date = 06/29/14 
 Pct Recovery = 129%  Analysis Date = 06/29/14 
 Pct Recovery = 129%  Analysis Date = 06/25/14 
 Pct Recovery = 129%  Analysis Date = 06/25/14 
 Pct Recovery = 129%  Analysis Date = 06/21/14 
 Pct Recovery = 129%  Analysis Date = 06/21/14 
 Pct Recovery = 129%  Analysis Date = 06/17/14 
 Pct Recovery = 129%  Analysis Date = 06/17/14 
 Pct Recovery = 129%  Analysis Date = 06/13/14 
 Pct Recovery = 129%  Analysis Date = 06/13/14 
 Pct Recovery = 129%  Analysis Date = 06/09/14 
 Pct Recovery = 129%  Analysis Date = 06/09/14 
 Pct Recovery = 129%  Analysis Date = 06/04/14 
 Pct Recovery = 129%  Analysis Date = 06/04/14 
 Pct Recovery = 129%  Analysis Date = 05/31/14 
 Pct Recovery = 129%  Analysis Date = 05/31/14 
 Pct Recovery = 129%  Analysis Date = 05/27/14 
 Pct Recovery = 129%  Analysis Date = 05/27/14 
 Pct Recovery = 129%  Analysis Date = 05/23/14 
 Pct Recovery = 129%  Analysis Date = 05/23/14 
 Pct Recovery = 129%  Analysis Date = 05/19/14 
 Pct Recovery = 129%  Analysis Date = 05/19/14 
 Pct Recovery = 129%  Analysis Date = 05/15/14 
 Pct Recovery = 129%  Analysis Date = 05/15/14 
 Pct Recovery = 129%  Analysis Date = 05/11/14 
 Pct Recovery = 129%  Analysis Date = 05/11/14 
 Pct Recovery = 129%  Analysis Date = 05/07/14 
 Pct Recovery = 129%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
ACETATE, PROPYL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 38 109% 24% 101% 23%
Total 38 109% 24% 101% 23%

Sample Statistics
ACETATE, PROPYL

Characteristic N % % Basis
Plotted 38 100% Spiked
Estimated Values 3 8% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 38 .  
False Negatives 0 0% 0 out of 38
Not Spiked 17 .  
False Positives 1 6% 1 out of 17

BQS OBSP Determination:
ACETONITRILE
METHOD: 4437 , TESTIDCODE: 76997GM016
Open Data Set

 Analysis Date = 06/23/16 
 SpikeMix = . 
 Pct Recovery = 216%  Analysis Date = 05/26/16 
 SpikeMix = Accu 216041354: 15 µl & NSI 041516: 15 µl & Accu 216041225: 15 µl 
 Pct Recovery = 216%  Analysis Date = 07/15/16 
 SpikeMix = Accu 216041354: 40 µl & NSI 041516: 40 µl & NSI 041416HVOC: 40 µl 
 Pct Recovery = 141%  Analysis Date = 07/29/16 
 SpikeMix = Supelco LC20145V: 40 µl & NSI 041516: 40 µl & NSI 041416HVOC: 40 µl 
 Pct Recovery = 127%  Analysis Date = 08/11/16 
 SpikeMix = Phenova B20160303: 25 µl & Supelco LC20145V: 25 µl & NSI 041416HVOC: 25 µl 
 Pct Recovery = 102%  Analysis Date = 05/26/16 
 SpikeMix = Supelco LC20145V: 25 µl & NSI 041516: 25 µl & NSI 041416HVOC: 25 µl 
 Pct Recovery = 106%  Analysis Date = 07/23/14 
 SpikeMix = Accu 214031128: 20 µl & Abs 032014: 20 µl 
 Pct Recovery = 110%  Analysis Date = 07/11/14 
 SpikeMix = ChemService 2615700: 20 µl & Accu 214031128: 20 µl 
 Pct Recovery = 101%  Analysis Date = 05/07/14 
 SpikeMix = NSI 031814: 20 µl & Accu 214031128: 20 µl 
 Pct Recovery = 114%  Analysis Date = 03/19/15 
 SpikeMix = Supelco LC06437: 20 µl & NSI 031814: 20 µl 
 Pct Recovery = 116%  Analysis Date = 08/20/14 
 SpikeMix = Supelco LC06437: 20 µl & Abs 032014: 20 µl 
 Pct Recovery = 101%  Analysis Date = 06/07/14 
 SpikeMix = ChemService 2615700: 20 µl & Supelco LC06437: 20 µl 
 Pct Recovery = 109%  Analysis Date = 01/22/16 
 SpikeMix = NSI 050515HVOC: 25 µl & ERA 0601-15-05: 25 µl 
 Pct Recovery = 107%  Analysis Date = 10/09/15 
 SpikeMix = Supelco LC13544: 25 µl & NSI 050515HVOC: 25 µl 
 Pct Recovery = 96%  Analysis Date = 06/25/15 
 SpikeMix = ChemService 3818700: 25 µl & NSI 050515HVOC: 25 µl 
 Pct Recovery = 97%  Analysis Date = 08/12/16 
 SpikeMix = Accu 216041354: 15 µl & Abs 060916HVOC: 15 µl 
 Pct Recovery = 154%  Analysis Date = 07/06/16 
 SpikeMix = Phenova B20160303: 15 µl & Accu 216041354: 15 µl & NSI 041416HVOC: 15 µl 
 Pct Recovery = 172%  Analysis Date = 07/27/16 
 SpikeMix = ChemService 5082800: 15 µl & Supelco LC20145V: 15 µl & Accu 216041225: 15 µl 
 Pct Recovery = 182%  Analysis Date = 11/25/15 
 SpikeMix = Accu 215041338: 15 µl & Abs 040315: 15 µl 
 Pct Recovery = 129%  Analysis Date = 09/24/15 
 SpikeMix = Abs 040315: 15 µl & ERA 0601-15-05: 15 µl 
 Pct Recovery = 100%  Analysis Date = 09/05/15 
 SpikeMix = Accu 215041338: 15 µl & NSI 050515HVOC: 15 µl 
 Pct Recovery = 88%  Analysis Date = 07/30/15 
 SpikeMix = Supelco LC13544: 15 µl & NSI 050515HVOC: 15 µl 
 Pct Recovery = 106%  Analysis Date = 06/16/15 
 SpikeMix = ChemService 3818700: 15 µl & NSI 050515HVOC: 15 µl 
 Pct Recovery = 101%  Analysis Date = 12/13/14 
 SpikeMix = Accu 214031128: 10 µl & NSI 031814: 10 µl 
 Pct Recovery = 108%  Analysis Date = 09/11/14 
 SpikeMix = Accu 214031128: 10 µl & Abs 032014: 10 µl 
 Pct Recovery = 110%  Analysis Date = 05/20/14 
 SpikeMix = ChemService 2615700: 10 µl & Accu 214031128: 10 µl 
 Pct Recovery = 92%  Analysis Date = 11/22/14 
 SpikeMix = ChemService 2615700: 10 µl & Supelco LC06437: 10 µl 
 Pct Recovery = 103%  Analysis Date = 06/17/14 
 SpikeMix = Supelco LC06437: 10 µl & Abs 032014: 10 µl 
 Pct Recovery = 100%  Analysis Date = 04/09/16 
 SpikeMix = Abs 040315: 10 µl & ChemService 3818700: 10 µl 
 Pct Recovery = 109%  Analysis Date = 01/05/16 
 SpikeMix = Accu 215041338: 10 µl & Abs 040315: 10 µl 
 Pct Recovery = 120%  Analysis Date = 10/23/15 
 SpikeMix = Abs 040315: 10 µl & ChemService 3818700: 10 µl 
 Pct Recovery = 116%  Analysis Date = 08/14/15 
 SpikeMix = Abs 040315: 10 µl & ERA 0601-15-05: 10 µl 
 Pct Recovery = 97%  Analysis Date = 05/05/15 
 SpikeMix = Supelco LC13544: 10 µl & Abs 040315: 10 µl 
 Pct Recovery = 115%  Analysis Date = 03/22/16 
 SpikeMix = Supelco LC13544: 10 µl & NSI 050515HVOC: 10 µl 
 Pct Recovery = 117%  Analysis Date = 12/05/15 
 SpikeMix = NSI 050515HVOC: 10 µl & ERA 0601-15-05: 10 µl 
 Pct Recovery = 94%  Analysis Date = 08/11/16 
 Pct Recovery = 158%  Analysis Date = 08/07/16 
 Pct Recovery = 158%  Analysis Date = 08/07/16 
 Pct Recovery = 158%  Analysis Date = 08/03/16 
 Pct Recovery = 157%  Analysis Date = 08/03/16 
 Pct Recovery = 157%  Analysis Date = 07/30/16 
 Pct Recovery = 156%  Analysis Date = 07/30/16 
 Pct Recovery = 156%  Analysis Date = 07/26/16 
 Pct Recovery = 155%  Analysis Date = 07/26/16 
 Pct Recovery = 155%  Analysis Date = 07/22/16 
 Pct Recovery = 155%  Analysis Date = 07/22/16 
 Pct Recovery = 155%  Analysis Date = 07/18/16 
 Pct Recovery = 154%  Analysis Date = 07/18/16 
 Pct Recovery = 154%  Analysis Date = 07/14/16 
 Pct Recovery = 153%  Analysis Date = 07/14/16 
 Pct Recovery = 153%  Analysis Date = 07/09/16 
 Pct Recovery = 152%  Analysis Date = 07/09/16 
 Pct Recovery = 152%  Analysis Date = 07/05/16 
 Pct Recovery = 151%  Analysis Date = 07/05/16 
 Pct Recovery = 151%  Analysis Date = 07/01/16 
 Pct Recovery = 151%  Analysis Date = 07/01/16 
 Pct Recovery = 151%  Analysis Date = 06/27/16 
 Pct Recovery = 150%  Analysis Date = 06/27/16 
 Pct Recovery = 150%  Analysis Date = 06/23/16 
 Pct Recovery = 149%  Analysis Date = 06/23/16 
 Pct Recovery = 149%  Analysis Date = 06/19/16 
 Pct Recovery = 148%  Analysis Date = 06/19/16 
 Pct Recovery = 148%  Analysis Date = 06/15/16 
 Pct Recovery = 148%  Analysis Date = 06/15/16 
 Pct Recovery = 148%  Analysis Date = 06/10/16 
 Pct Recovery = 147%  Analysis Date = 06/10/16 
 Pct Recovery = 147%  Analysis Date = 06/06/16 
 Pct Recovery = 146%  Analysis Date = 06/06/16 
 Pct Recovery = 146%  Analysis Date = 06/02/16 
 Pct Recovery = 145%  Analysis Date = 06/02/16 
 Pct Recovery = 145%  Analysis Date = 05/29/16 
 Pct Recovery = 145%  Analysis Date = 05/29/16 
 Pct Recovery = 145%  Analysis Date = 05/25/16 
 Pct Recovery = 144%  Analysis Date = 05/25/16 
 Pct Recovery = 144%  Analysis Date = 05/21/16 
 Pct Recovery = 143%  Analysis Date = 05/21/16 
 Pct Recovery = 143%  Analysis Date = 05/17/16 
 Pct Recovery = 142%  Analysis Date = 05/17/16 
 Pct Recovery = 142%  Analysis Date = 05/12/16 
 Pct Recovery = 141%  Analysis Date = 05/12/16 
 Pct Recovery = 141%  Analysis Date = 05/08/16 
 Pct Recovery = 140%  Analysis Date = 05/08/16 
 Pct Recovery = 140%  Analysis Date = 05/04/16 
 Pct Recovery = 140%  Analysis Date = 05/04/16 
 Pct Recovery = 140%  Analysis Date = 04/30/16 
 Pct Recovery = 139%  Analysis Date = 04/30/16 
 Pct Recovery = 139%  Analysis Date = 04/26/16 
 Pct Recovery = 138%  Analysis Date = 04/26/16 
 Pct Recovery = 138%  Analysis Date = 04/22/16 
 Pct Recovery = 137%  Analysis Date = 04/22/16 
 Pct Recovery = 137%  Analysis Date = 04/18/16 
 Pct Recovery = 136%  Analysis Date = 04/18/16 
 Pct Recovery = 136%  Analysis Date = 04/13/16 
 Pct Recovery = 135%  Analysis Date = 04/13/16 
 Pct Recovery = 135%  Analysis Date = 04/09/16 
 Pct Recovery = 135%  Analysis Date = 04/09/16 
 Pct Recovery = 135%  Analysis Date = 04/05/16 
 Pct Recovery = 134%  Analysis Date = 04/05/16 
 Pct Recovery = 134%  Analysis Date = 04/01/16 
 Pct Recovery = 133%  Analysis Date = 04/01/16 
 Pct Recovery = 133%  Analysis Date = 03/28/16 
 Pct Recovery = 132%  Analysis Date = 03/28/16 
 Pct Recovery = 132%  Analysis Date = 03/24/16 
 Pct Recovery = 131%  Analysis Date = 03/24/16 
 Pct Recovery = 131%  Analysis Date = 03/20/16 
 Pct Recovery = 130%  Analysis Date = 03/20/16 
 Pct Recovery = 130%  Analysis Date = 03/15/16 
 Pct Recovery = 130%  Analysis Date = 03/15/16 
 Pct Recovery = 130%  Analysis Date = 03/11/16 
 Pct Recovery = 129%  Analysis Date = 03/11/16 
 Pct Recovery = 129%  Analysis Date = 03/07/16 
 Pct Recovery = 128%  Analysis Date = 03/07/16 
 Pct Recovery = 128%  Analysis Date = 03/03/16 
 Pct Recovery = 127%  Analysis Date = 03/03/16 
 Pct Recovery = 127%  Analysis Date = 02/28/16 
 Pct Recovery = 126%  Analysis Date = 02/28/16 
 Pct Recovery = 126%  Analysis Date = 02/24/16 
 Pct Recovery = 125%  Analysis Date = 02/24/16 
 Pct Recovery = 125%  Analysis Date = 02/20/16 
 Pct Recovery = 125%  Analysis Date = 02/20/16 
 Pct Recovery = 125%  Analysis Date = 02/15/16 
 Pct Recovery = 124%  Analysis Date = 02/15/16 
 Pct Recovery = 124%  Analysis Date = 02/11/16 
 Pct Recovery = 123%  Analysis Date = 02/11/16 
 Pct Recovery = 123%  Analysis Date = 02/07/16 
 Pct Recovery = 122%  Analysis Date = 02/07/16 
 Pct Recovery = 122%  Analysis Date = 02/03/16 
 Pct Recovery = 121%  Analysis Date = 02/03/16 
 Pct Recovery = 121%  Analysis Date = 01/30/16 
 Pct Recovery = 120%  Analysis Date = 01/30/16 
 Pct Recovery = 120%  Analysis Date = 01/26/16 
 Pct Recovery = 120%  Analysis Date = 01/26/16 
 Pct Recovery = 120%  Analysis Date = 01/22/16 
 Pct Recovery = 119%  Analysis Date = 01/22/16 
 Pct Recovery = 119%  Analysis Date = 01/17/16 
 Pct Recovery = 118%  Analysis Date = 01/17/16 
 Pct Recovery = 118%  Analysis Date = 01/13/16 
 Pct Recovery = 117%  Analysis Date = 01/13/16 
 Pct Recovery = 117%  Analysis Date = 01/09/16 
 Pct Recovery = 116%  Analysis Date = 01/09/16 
 Pct Recovery = 116%  Analysis Date = 01/05/16 
 Pct Recovery = 115%  Analysis Date = 01/05/16 
 Pct Recovery = 115%  Analysis Date = 01/01/16 
 Pct Recovery = 115%  Analysis Date = 01/01/16 
 Pct Recovery = 115%  Analysis Date = 12/28/15 
 Pct Recovery = 114%  Analysis Date = 12/28/15 
 Pct Recovery = 114%  Analysis Date = 12/24/15 
 Pct Recovery = 114%  Analysis Date = 12/24/15 
 Pct Recovery = 114%  Analysis Date = 12/20/15 
 Pct Recovery = 113%  Analysis Date = 12/20/15 
 Pct Recovery = 113%  Analysis Date = 12/15/15 
 Pct Recovery = 113%  Analysis Date = 12/15/15 
 Pct Recovery = 113%  Analysis Date = 12/11/15 
 Pct Recovery = 112%  Analysis Date = 12/11/15 
 Pct Recovery = 112%  Analysis Date = 12/07/15 
 Pct Recovery = 112%  Analysis Date = 12/07/15 
 Pct Recovery = 112%  Analysis Date = 12/03/15 
 Pct Recovery = 111%  Analysis Date = 12/03/15 
 Pct Recovery = 111%  Analysis Date = 11/29/15 
 Pct Recovery = 110%  Analysis Date = 11/29/15 
 Pct Recovery = 110%  Analysis Date = 11/25/15 
 Pct Recovery = 110%  Analysis Date = 11/25/15 
 Pct Recovery = 110%  Analysis Date = 11/21/15 
 Pct Recovery = 110%  Analysis Date = 11/21/15 
 Pct Recovery = 110%  Analysis Date = 11/16/15 
 Pct Recovery = 109%  Analysis Date = 11/16/15 
 Pct Recovery = 109%  Analysis Date = 11/12/15 
 Pct Recovery = 109%  Analysis Date = 11/12/15 
 Pct Recovery = 109%  Analysis Date = 11/08/15 
 Pct Recovery = 109%  Analysis Date = 11/08/15 
 Pct Recovery = 109%  Analysis Date = 11/04/15 
 Pct Recovery = 108%  Analysis Date = 11/04/15 
 Pct Recovery = 108%  Analysis Date = 10/31/15 
 Pct Recovery = 108%  Analysis Date = 10/31/15 
 Pct Recovery = 108%  Analysis Date = 10/27/15 
 Pct Recovery = 108%  Analysis Date = 10/27/15 
 Pct Recovery = 108%  Analysis Date = 10/23/15 
 Pct Recovery = 108%  Analysis Date = 10/23/15 
 Pct Recovery = 108%  Analysis Date = 10/18/15 
 Pct Recovery = 107%  Analysis Date = 10/18/15 
 Pct Recovery = 107%  Analysis Date = 10/14/15 
 Pct Recovery = 107%  Analysis Date = 10/14/15 
 Pct Recovery = 107%  Analysis Date = 10/10/15 
 Pct Recovery = 107%  Analysis Date = 10/10/15 
 Pct Recovery = 107%  Analysis Date = 10/06/15 
 Pct Recovery = 106%  Analysis Date = 10/06/15 
 Pct Recovery = 106%  Analysis Date = 10/02/15 
 Pct Recovery = 106%  Analysis Date = 10/02/15 
 Pct Recovery = 106%  Analysis Date = 09/28/15 
 Pct Recovery = 106%  Analysis Date = 09/28/15 
 Pct Recovery = 106%  Analysis Date = 09/24/15 
 Pct Recovery = 106%  Analysis Date = 09/24/15 
 Pct Recovery = 106%  Analysis Date = 09/19/15 
 Pct Recovery = 106%  Analysis Date = 09/19/15 
 Pct Recovery = 106%  Analysis Date = 09/15/15 
 Pct Recovery = 106%  Analysis Date = 09/15/15 
 Pct Recovery = 106%  Analysis Date = 09/11/15 
 Pct Recovery = 106%  Analysis Date = 09/11/15 
 Pct Recovery = 106%  Analysis Date = 09/07/15 
 Pct Recovery = 105%  Analysis Date = 09/07/15 
 Pct Recovery = 105%  Analysis Date = 09/03/15 
 Pct Recovery = 105%  Analysis Date = 09/03/15 
 Pct Recovery = 105%  Analysis Date = 08/30/15 
 Pct Recovery = 105%  Analysis Date = 08/30/15 
 Pct Recovery = 105%  Analysis Date = 08/26/15 
 Pct Recovery = 105%  Analysis Date = 08/26/15 
 Pct Recovery = 105%  Analysis Date = 08/21/15 
 Pct Recovery = 105%  Analysis Date = 08/21/15 
 Pct Recovery = 105%  Analysis Date = 08/17/15 
 Pct Recovery = 105%  Analysis Date = 08/17/15 
 Pct Recovery = 105%  Analysis Date = 08/13/15 
 Pct Recovery = 105%  Analysis Date = 08/13/15 
 Pct Recovery = 105%  Analysis Date = 08/09/15 
 Pct Recovery = 105%  Analysis Date = 08/09/15 
 Pct Recovery = 105%  Analysis Date = 08/05/15 
 Pct Recovery = 105%  Analysis Date = 08/05/15 
 Pct Recovery = 105%  Analysis Date = 08/01/15 
 Pct Recovery = 105%  Analysis Date = 08/01/15 
 Pct Recovery = 105%  Analysis Date = 07/28/15 
 Pct Recovery = 105%  Analysis Date = 07/28/15 
 Pct Recovery = 105%  Analysis Date = 07/23/15 
 Pct Recovery = 105%  Analysis Date = 07/23/15 
 Pct Recovery = 105%  Analysis Date = 07/19/15 
 Pct Recovery = 105%  Analysis Date = 07/19/15 
 Pct Recovery = 105%  Analysis Date = 07/15/15 
 Pct Recovery = 105%  Analysis Date = 07/15/15 
 Pct Recovery = 105%  Analysis Date = 07/11/15 
 Pct Recovery = 105%  Analysis Date = 07/11/15 
 Pct Recovery = 105%  Analysis Date = 07/07/15 
 Pct Recovery = 105%  Analysis Date = 07/07/15 
 Pct Recovery = 105%  Analysis Date = 07/03/15 
 Pct Recovery = 105%  Analysis Date = 07/03/15 
 Pct Recovery = 105%  Analysis Date = 06/29/15 
 Pct Recovery = 105%  Analysis Date = 06/29/15 
 Pct Recovery = 105%  Analysis Date = 06/24/15 
 Pct Recovery = 105%  Analysis Date = 06/24/15 
 Pct Recovery = 105%  Analysis Date = 06/20/15 
 Pct Recovery = 105%  Analysis Date = 06/20/15 
 Pct Recovery = 105%  Analysis Date = 06/16/15 
 Pct Recovery = 105%  Analysis Date = 06/16/15 
 Pct Recovery = 105%  Analysis Date = 06/12/15 
 Pct Recovery = 105%  Analysis Date = 06/12/15 
 Pct Recovery = 105%  Analysis Date = 06/08/15 
 Pct Recovery = 105%  Analysis Date = 06/08/15 
 Pct Recovery = 105%  Analysis Date = 06/04/15 
 Pct Recovery = 105%  Analysis Date = 06/04/15 
 Pct Recovery = 105%  Analysis Date = 05/31/15 
 Pct Recovery = 105%  Analysis Date = 05/31/15 
 Pct Recovery = 105%  Analysis Date = 05/27/15 
 Pct Recovery = 105%  Analysis Date = 05/27/15 
 Pct Recovery = 105%  Analysis Date = 05/22/15 
 Pct Recovery = 105%  Analysis Date = 05/22/15 
 Pct Recovery = 105%  Analysis Date = 05/18/15 
 Pct Recovery = 105%  Analysis Date = 05/18/15 
 Pct Recovery = 105%  Analysis Date = 05/14/15 
 Pct Recovery = 105%  Analysis Date = 05/14/15 
 Pct Recovery = 105%  Analysis Date = 05/10/15 
 Pct Recovery = 105%  Analysis Date = 05/10/15 
 Pct Recovery = 105%  Analysis Date = 05/06/15 
 Pct Recovery = 105%  Analysis Date = 05/06/15 
 Pct Recovery = 105%  Analysis Date = 05/02/15 
 Pct Recovery = 105%  Analysis Date = 05/02/15 
 Pct Recovery = 105%  Analysis Date = 04/28/15 
 Pct Recovery = 105%  Analysis Date = 04/28/15 
 Pct Recovery = 105%  Analysis Date = 04/23/15 
 Pct Recovery = 105%  Analysis Date = 04/23/15 
 Pct Recovery = 105%  Analysis Date = 04/19/15 
 Pct Recovery = 105%  Analysis Date = 04/19/15 
 Pct Recovery = 105%  Analysis Date = 04/15/15 
 Pct Recovery = 105%  Analysis Date = 04/15/15 
 Pct Recovery = 105%  Analysis Date = 04/11/15 
 Pct Recovery = 105%  Analysis Date = 04/11/15 
 Pct Recovery = 105%  Analysis Date = 04/07/15 
 Pct Recovery = 105%  Analysis Date = 04/07/15 
 Pct Recovery = 105%  Analysis Date = 04/03/15 
 Pct Recovery = 105%  Analysis Date = 04/03/15 
 Pct Recovery = 105%  Analysis Date = 03/30/15 
 Pct Recovery = 105%  Analysis Date = 03/30/15 
 Pct Recovery = 105%  Analysis Date = 03/25/15 
 Pct Recovery = 105%  Analysis Date = 03/25/15 
 Pct Recovery = 105%  Analysis Date = 03/21/15 
 Pct Recovery = 105%  Analysis Date = 03/21/15 
 Pct Recovery = 105%  Analysis Date = 03/17/15 
 Pct Recovery = 105%  Analysis Date = 03/17/15 
 Pct Recovery = 105%  Analysis Date = 03/13/15 
 Pct Recovery = 105%  Analysis Date = 03/13/15 
 Pct Recovery = 105%  Analysis Date = 03/09/15 
 Pct Recovery = 105%  Analysis Date = 03/09/15 
 Pct Recovery = 105%  Analysis Date = 03/05/15 
 Pct Recovery = 105%  Analysis Date = 03/05/15 
 Pct Recovery = 105%  Analysis Date = 03/01/15 
 Pct Recovery = 105%  Analysis Date = 03/01/15 
 Pct Recovery = 105%  Analysis Date = 02/24/15 
 Pct Recovery = 105%  Analysis Date = 02/24/15 
 Pct Recovery = 105%  Analysis Date = 02/20/15 
 Pct Recovery = 105%  Analysis Date = 02/20/15 
 Pct Recovery = 105%  Analysis Date = 02/16/15 
 Pct Recovery = 105%  Analysis Date = 02/16/15 
 Pct Recovery = 105%  Analysis Date = 02/12/15 
 Pct Recovery = 105%  Analysis Date = 02/12/15 
 Pct Recovery = 105%  Analysis Date = 02/08/15 
 Pct Recovery = 105%  Analysis Date = 02/08/15 
 Pct Recovery = 105%  Analysis Date = 02/04/15 
 Pct Recovery = 105%  Analysis Date = 02/04/15 
 Pct Recovery = 105%  Analysis Date = 01/31/15 
 Pct Recovery = 105%  Analysis Date = 01/31/15 
 Pct Recovery = 105%  Analysis Date = 01/26/15 
 Pct Recovery = 105%  Analysis Date = 01/26/15 
 Pct Recovery = 105%  Analysis Date = 01/22/15 
 Pct Recovery = 105%  Analysis Date = 01/22/15 
 Pct Recovery = 105%  Analysis Date = 01/18/15 
 Pct Recovery = 105%  Analysis Date = 01/18/15 
 Pct Recovery = 105%  Analysis Date = 01/14/15 
 Pct Recovery = 105%  Analysis Date = 01/14/15 
 Pct Recovery = 105%  Analysis Date = 01/10/15 
 Pct Recovery = 105%  Analysis Date = 01/10/15 
 Pct Recovery = 105%  Analysis Date = 01/06/15 
 Pct Recovery = 105%  Analysis Date = 01/06/15 
 Pct Recovery = 105%  Analysis Date = 01/02/15 
 Pct Recovery = 105%  Analysis Date = 01/02/15 
 Pct Recovery = 105%  Analysis Date = 12/28/14 
 Pct Recovery = 105%  Analysis Date = 12/28/14 
 Pct Recovery = 105%  Analysis Date = 12/24/14 
 Pct Recovery = 105%  Analysis Date = 12/24/14 
 Pct Recovery = 105%  Analysis Date = 12/20/14 
 Pct Recovery = 105%  Analysis Date = 12/20/14 
 Pct Recovery = 105%  Analysis Date = 12/16/14 
 Pct Recovery = 105%  Analysis Date = 12/16/14 
 Pct Recovery = 105%  Analysis Date = 12/12/14 
 Pct Recovery = 105%  Analysis Date = 12/12/14 
 Pct Recovery = 105%  Analysis Date = 12/08/14 
 Pct Recovery = 105%  Analysis Date = 12/08/14 
 Pct Recovery = 105%  Analysis Date = 12/04/14 
 Pct Recovery = 105%  Analysis Date = 12/04/14 
 Pct Recovery = 105%  Analysis Date = 11/29/14 
 Pct Recovery = 105%  Analysis Date = 11/29/14 
 Pct Recovery = 105%  Analysis Date = 11/25/14 
 Pct Recovery = 105%  Analysis Date = 11/25/14 
 Pct Recovery = 105%  Analysis Date = 11/21/14 
 Pct Recovery = 105%  Analysis Date = 11/21/14 
 Pct Recovery = 105%  Analysis Date = 11/17/14 
 Pct Recovery = 105%  Analysis Date = 11/17/14 
 Pct Recovery = 105%  Analysis Date = 11/13/14 
 Pct Recovery = 105%  Analysis Date = 11/13/14 
 Pct Recovery = 105%  Analysis Date = 11/09/14 
 Pct Recovery = 105%  Analysis Date = 11/09/14 
 Pct Recovery = 105%  Analysis Date = 11/05/14 
 Pct Recovery = 105%  Analysis Date = 11/05/14 
 Pct Recovery = 105%  Analysis Date = 11/01/14 
 Pct Recovery = 105%  Analysis Date = 11/01/14 
 Pct Recovery = 105%  Analysis Date = 10/27/14 
 Pct Recovery = 105%  Analysis Date = 10/27/14 
 Pct Recovery = 105%  Analysis Date = 10/23/14 
 Pct Recovery = 105%  Analysis Date = 10/23/14 
 Pct Recovery = 105%  Analysis Date = 10/19/14 
 Pct Recovery = 105%  Analysis Date = 10/19/14 
 Pct Recovery = 105%  Analysis Date = 10/15/14 
 Pct Recovery = 105%  Analysis Date = 10/15/14 
 Pct Recovery = 105%  Analysis Date = 10/11/14 
 Pct Recovery = 105%  Analysis Date = 10/11/14 
 Pct Recovery = 105%  Analysis Date = 10/07/14 
 Pct Recovery = 105%  Analysis Date = 10/07/14 
 Pct Recovery = 105%  Analysis Date = 10/03/14 
 Pct Recovery = 105%  Analysis Date = 10/03/14 
 Pct Recovery = 105%  Analysis Date = 09/28/14 
 Pct Recovery = 105%  Analysis Date = 09/28/14 
 Pct Recovery = 105%  Analysis Date = 09/24/14 
 Pct Recovery = 105%  Analysis Date = 09/24/14 
 Pct Recovery = 105%  Analysis Date = 09/20/14 
 Pct Recovery = 105%  Analysis Date = 09/20/14 
 Pct Recovery = 105%  Analysis Date = 09/16/14 
 Pct Recovery = 105%  Analysis Date = 09/16/14 
 Pct Recovery = 105%  Analysis Date = 09/12/14 
 Pct Recovery = 105%  Analysis Date = 09/12/14 
 Pct Recovery = 105%  Analysis Date = 09/08/14 
 Pct Recovery = 105%  Analysis Date = 09/08/14 
 Pct Recovery = 105%  Analysis Date = 09/04/14 
 Pct Recovery = 105%  Analysis Date = 09/04/14 
 Pct Recovery = 105%  Analysis Date = 08/30/14 
 Pct Recovery = 105%  Analysis Date = 08/30/14 
 Pct Recovery = 105%  Analysis Date = 08/26/14 
 Pct Recovery = 105%  Analysis Date = 08/26/14 
 Pct Recovery = 105%  Analysis Date = 08/22/14 
 Pct Recovery = 105%  Analysis Date = 08/22/14 
 Pct Recovery = 105%  Analysis Date = 08/18/14 
 Pct Recovery = 105%  Analysis Date = 08/18/14 
 Pct Recovery = 105%  Analysis Date = 08/14/14 
 Pct Recovery = 105%  Analysis Date = 08/14/14 
 Pct Recovery = 105%  Analysis Date = 08/10/14 
 Pct Recovery = 105%  Analysis Date = 08/10/14 
 Pct Recovery = 105%  Analysis Date = 08/06/14 
 Pct Recovery = 105%  Analysis Date = 08/06/14 
 Pct Recovery = 105%  Analysis Date = 08/01/14 
 Pct Recovery = 105%  Analysis Date = 08/01/14 
 Pct Recovery = 105%  Analysis Date = 07/28/14 
 Pct Recovery = 105%  Analysis Date = 07/28/14 
 Pct Recovery = 105%  Analysis Date = 07/24/14 
 Pct Recovery = 105%  Analysis Date = 07/24/14 
 Pct Recovery = 105%  Analysis Date = 07/20/14 
 Pct Recovery = 105%  Analysis Date = 07/20/14 
 Pct Recovery = 105%  Analysis Date = 07/16/14 
 Pct Recovery = 105%  Analysis Date = 07/16/14 
 Pct Recovery = 105%  Analysis Date = 07/12/14 
 Pct Recovery = 105%  Analysis Date = 07/12/14 
 Pct Recovery = 105%  Analysis Date = 07/08/14 
 Pct Recovery = 105%  Analysis Date = 07/08/14 
 Pct Recovery = 105%  Analysis Date = 07/03/14 
 Pct Recovery = 105%  Analysis Date = 07/03/14 
 Pct Recovery = 105%  Analysis Date = 06/29/14 
 Pct Recovery = 105%  Analysis Date = 06/29/14 
 Pct Recovery = 105%  Analysis Date = 06/25/14 
 Pct Recovery = 105%  Analysis Date = 06/25/14 
 Pct Recovery = 105%  Analysis Date = 06/21/14 
 Pct Recovery = 105%  Analysis Date = 06/21/14 
 Pct Recovery = 105%  Analysis Date = 06/17/14 
 Pct Recovery = 105%  Analysis Date = 06/17/14 
 Pct Recovery = 105%  Analysis Date = 06/13/14 
 Pct Recovery = 105%  Analysis Date = 06/13/14 
 Pct Recovery = 105%  Analysis Date = 06/09/14 
 Pct Recovery = 105%  Analysis Date = 06/09/14 
 Pct Recovery = 105%  Analysis Date = 06/04/14 
 Pct Recovery = 105%  Analysis Date = 06/04/14 
 Pct Recovery = 105%  Analysis Date = 05/31/14 
 Pct Recovery = 105%  Analysis Date = 05/31/14 
 Pct Recovery = 105%  Analysis Date = 05/27/14 
 Pct Recovery = 104%  Analysis Date = 05/27/14 
 Pct Recovery = 104%  Analysis Date = 05/23/14 
 Pct Recovery = 104%  Analysis Date = 05/23/14 
 Pct Recovery = 104%  Analysis Date = 05/19/14 
 Pct Recovery = 104%  Analysis Date = 05/19/14 
 Pct Recovery = 104%  Analysis Date = 05/15/14 
 Pct Recovery = 104%  Analysis Date = 05/15/14 
 Pct Recovery = 104%  Analysis Date = 05/11/14 
 Pct Recovery = 104%  Analysis Date = 05/11/14 
 Pct Recovery = 104%  Analysis Date = 05/07/14 
 Pct Recovery = 104%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
ACETONITRILE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 35 119% 32% 109% 14%
Total 35 119% 32% 109% 14%

Sample Statistics
ACETONITRILE

Characteristic N % % Basis
Plotted 35 100% Spiked
Estimated Values 1 3% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 35 .  
False Negatives 0 0% 0 out of 35
Not Spiked 15 .  
False Positives 5 33% 5 out of 15

BQS OBSP Determination:
ACROLEIN
METHOD: 4437 , TESTIDCODE: 34210GM016
Open Data Set

 Analysis Date = 06/07/14 
 SpikeMix = ChemService 2615700: 20 µl & Supelco LC06437: 20 µl 
 Pct Recovery = 278%  Analysis Date = 01/22/16 
 SpikeMix = NSI 050515HVOC: 25 µl & ERA 0601-15-05: 25 µl 
 Pct Recovery = 127%  Analysis Date = 10/09/15 
 SpikeMix = Supelco LC13544: 25 µl & NSI 050515HVOC: 25 µl 
 Pct Recovery = 104%  Analysis Date = 06/25/15 
 SpikeMix = ChemService 3818700: 25 µl & NSI 050515HVOC: 25 µl 
 Pct Recovery = 80%  Analysis Date = 09/05/15 
 SpikeMix = Accu 215041338: 15 µl & NSI 050515HVOC: 15 µl 
 Pct Recovery = 131%  Analysis Date = 07/30/15 
 SpikeMix = Supelco LC13544: 15 µl & NSI 050515HVOC: 15 µl 
 Pct Recovery = 82%  Analysis Date = 06/16/15 
 SpikeMix = ChemService 3818700: 15 µl & NSI 050515HVOC: 15 µl 
 Pct Recovery = 69%  Analysis Date = 03/22/16 
 SpikeMix = Supelco LC13544: 10 µl & NSI 050515HVOC: 10 µl 
 Pct Recovery = 50%  Analysis Date = 12/05/15 
 SpikeMix = NSI 050515HVOC: 10 µl & ERA 0601-15-05: 10 µl 
 Pct Recovery = 117%  Analysis Date = 08/20/14 
 SpikeMix = Supelco LC06437: 20 µl & Abs 032014: 20 µl 
 Pct Recovery = 70%  Analysis Date = 09/06/14 
 SpikeMix = ERA 0321-14-05: 10 µl & Supelco LC06437: 10 µl 
 Pct Recovery = 92%  Analysis Date = 06/17/14 
 SpikeMix = Supelco LC06437: 10 µl & Abs 032014: 10 µl 
 Pct Recovery = 102%  Analysis Date = 03/19/15 
 SpikeMix = Supelco LC06437: 20 µl & NSI 031814: 20 µl 
 Pct Recovery = 21%  Analysis Date = 03/22/16 
 Pct Recovery = 74%  Analysis Date = 03/18/16 
 Pct Recovery = 75%  Analysis Date = 03/18/16 
 Pct Recovery = 75%  Analysis Date = 03/15/16 
 Pct Recovery = 76%  Analysis Date = 03/15/16 
 Pct Recovery = 76%  Analysis Date = 03/12/16 
 Pct Recovery = 77%  Analysis Date = 03/12/16 
 Pct Recovery = 77%  Analysis Date = 03/08/16 
 Pct Recovery = 79%  Analysis Date = 03/08/16 
 Pct Recovery = 79%  Analysis Date = 03/05/16 
 Pct Recovery = 80%  Analysis Date = 03/05/16 
 Pct Recovery = 80%  Analysis Date = 03/02/16 
 Pct Recovery = 81%  Analysis Date = 03/02/16 
 Pct Recovery = 81%  Analysis Date = 02/28/16 
 Pct Recovery = 82%  Analysis Date = 02/28/16 
 Pct Recovery = 82%  Analysis Date = 02/24/16 
 Pct Recovery = 83%  Analysis Date = 02/24/16 
 Pct Recovery = 83%  Analysis Date = 02/21/16 
 Pct Recovery = 84%  Analysis Date = 02/21/16 
 Pct Recovery = 84%  Analysis Date = 02/18/16 
 Pct Recovery = 85%  Analysis Date = 02/18/16 
 Pct Recovery = 85%  Analysis Date = 02/15/16 
 Pct Recovery = 86%  Analysis Date = 02/15/16 
 Pct Recovery = 86%  Analysis Date = 02/11/16 
 Pct Recovery = 87%  Analysis Date = 02/11/16 
 Pct Recovery = 87%  Analysis Date = 02/08/16 
 Pct Recovery = 88%  Analysis Date = 02/08/16 
 Pct Recovery = 88%  Analysis Date = 02/05/16 
 Pct Recovery = 89%  Analysis Date = 02/05/16 
 Pct Recovery = 89%  Analysis Date = 02/01/16 
 Pct Recovery = 90%  Analysis Date = 02/01/16 
 Pct Recovery = 90%  Analysis Date = 01/29/16 
 Pct Recovery = 91%  Analysis Date = 01/29/16 
 Pct Recovery = 91%  Analysis Date = 01/26/16 
 Pct Recovery = 92%  Analysis Date = 01/26/16 
 Pct Recovery = 92%  Analysis Date = 01/23/16 
 Pct Recovery = 94%  Analysis Date = 01/23/16 
 Pct Recovery = 94%  Analysis Date = 01/19/16 
 Pct Recovery = 95%  Analysis Date = 01/19/16 
 Pct Recovery = 95%  Analysis Date = 01/16/16 
 Pct Recovery = 96%  Analysis Date = 01/16/16 
 Pct Recovery = 96%  Analysis Date = 01/13/16 
 Pct Recovery = 97%  Analysis Date = 01/13/16 
 Pct Recovery = 97%  Analysis Date = 01/10/16 
 Pct Recovery = 98%  Analysis Date = 01/10/16 
 Pct Recovery = 98%  Analysis Date = 01/06/16 
 Pct Recovery = 99%  Analysis Date = 01/06/16 
 Pct Recovery = 99%  Analysis Date = 01/03/16 
 Pct Recovery = 100%  Analysis Date = 01/03/16 
 Pct Recovery = 100%  Analysis Date = 12/31/15 
 Pct Recovery = 101%  Analysis Date = 12/31/15 
 Pct Recovery = 101%  Analysis Date = 12/27/15 
 Pct Recovery = 102%  Analysis Date = 12/27/15 
 Pct Recovery = 102%  Analysis Date = 12/24/15 
 Pct Recovery = 103%  Analysis Date = 12/24/15 
 Pct Recovery = 103%  Analysis Date = 12/21/15 
 Pct Recovery = 104%  Analysis Date = 12/21/15 
 Pct Recovery = 104%  Analysis Date = 12/18/15 
 Pct Recovery = 105%  Analysis Date = 12/18/15 
 Pct Recovery = 105%  Analysis Date = 12/14/15 
 Pct Recovery = 107%  Analysis Date = 12/14/15 
 Pct Recovery = 107%  Analysis Date = 12/11/15 
 Pct Recovery = 108%  Analysis Date = 12/11/15 
 Pct Recovery = 108%  Analysis Date = 12/08/15 
 Pct Recovery = 109%  Analysis Date = 12/08/15 
 Pct Recovery = 109%  Analysis Date = 12/05/15 
 Pct Recovery = 110%  Analysis Date = 12/05/15 
 Pct Recovery = 110%  Analysis Date = 12/01/15 
 Pct Recovery = 110%  Analysis Date = 12/01/15 
 Pct Recovery = 110%  Analysis Date = 11/28/15 
 Pct Recovery = 110%  Analysis Date = 11/28/15 
 Pct Recovery = 110%  Analysis Date = 11/25/15 
 Pct Recovery = 110%  Analysis Date = 11/25/15 
 Pct Recovery = 110%  Analysis Date = 11/22/15 
 Pct Recovery = 110%  Analysis Date = 11/22/15 
 Pct Recovery = 110%  Analysis Date = 11/18/15 
 Pct Recovery = 111%  Analysis Date = 11/18/15 
 Pct Recovery = 111%  Analysis Date = 11/15/15 
 Pct Recovery = 111%  Analysis Date = 11/15/15 
 Pct Recovery = 111%  Analysis Date = 11/12/15 
 Pct Recovery = 111%  Analysis Date = 11/12/15 
 Pct Recovery = 111%  Analysis Date = 11/08/15 
 Pct Recovery = 111%  Analysis Date = 11/08/15 
 Pct Recovery = 111%  Analysis Date = 11/05/15 
 Pct Recovery = 111%  Analysis Date = 11/05/15 
 Pct Recovery = 111%  Analysis Date = 11/02/15 
 Pct Recovery = 111%  Analysis Date = 11/02/15 
 Pct Recovery = 111%  Analysis Date = 10/30/15 
 Pct Recovery = 112%  Analysis Date = 10/30/15 
 Pct Recovery = 112%  Analysis Date = 10/26/15 
 Pct Recovery = 112%  Analysis Date = 10/26/15 
 Pct Recovery = 112%  Analysis Date = 10/23/15 
 Pct Recovery = 112%  Analysis Date = 10/23/15 
 Pct Recovery = 112%  Analysis Date = 10/20/15 
 Pct Recovery = 112%  Analysis Date = 10/20/15 
 Pct Recovery = 112%  Analysis Date = 10/17/15 
 Pct Recovery = 112%  Analysis Date = 10/17/15 
 Pct Recovery = 112%  Analysis Date = 10/13/15 
 Pct Recovery = 112%  Analysis Date = 10/13/15 
 Pct Recovery = 112%  Analysis Date = 10/10/15 
 Pct Recovery = 113%  Analysis Date = 10/10/15 
 Pct Recovery = 113%  Analysis Date = 10/07/15 
 Pct Recovery = 112%  Analysis Date = 10/07/15 
 Pct Recovery = 112%  Analysis Date = 10/03/15 
 Pct Recovery = 111%  Analysis Date = 10/03/15 
 Pct Recovery = 111%  Analysis Date = 09/30/15 
 Pct Recovery = 110%  Analysis Date = 09/30/15 
 Pct Recovery = 110%  Analysis Date = 09/27/15 
 Pct Recovery = 109%  Analysis Date = 09/27/15 
 Pct Recovery = 109%  Analysis Date = 09/24/15 
 Pct Recovery = 108%  Analysis Date = 09/24/15 
 Pct Recovery = 108%  Analysis Date = 09/20/15 
 Pct Recovery = 107%  Analysis Date = 09/20/15 
 Pct Recovery = 107%  Analysis Date = 09/17/15 
 Pct Recovery = 106%  Analysis Date = 09/17/15 
 Pct Recovery = 106%  Analysis Date = 09/14/15 
 Pct Recovery = 106%  Analysis Date = 09/14/15 
 Pct Recovery = 106%  Analysis Date = 09/11/15 
 Pct Recovery = 105%  Analysis Date = 09/11/15 
 Pct Recovery = 105%  Analysis Date = 09/07/15 
 Pct Recovery = 104%  Analysis Date = 09/07/15 
 Pct Recovery = 104%  Analysis Date = 09/04/15 
 Pct Recovery = 103%  Analysis Date = 09/04/15 
 Pct Recovery = 103%  Analysis Date = 09/01/15 
 Pct Recovery = 102%  Analysis Date = 09/01/15 
 Pct Recovery = 102%  Analysis Date = 08/28/15 
 Pct Recovery = 101%  Analysis Date = 08/28/15 
 Pct Recovery = 101%  Analysis Date = 08/25/15 
 Pct Recovery = 100%  Analysis Date = 08/25/15 
 Pct Recovery = 100%  Analysis Date = 08/22/15 
 Pct Recovery = 99%  Analysis Date = 08/22/15 
 Pct Recovery = 99%  Analysis Date = 08/19/15 
 Pct Recovery = 98%  Analysis Date = 08/19/15 
 Pct Recovery = 98%  Analysis Date = 08/15/15 
 Pct Recovery = 97%  Analysis Date = 08/15/15 
 Pct Recovery = 97%  Analysis Date = 08/12/15 
 Pct Recovery = 96%  Analysis Date = 08/12/15 
 Pct Recovery = 96%  Analysis Date = 08/09/15 
 Pct Recovery = 95%  Analysis Date = 08/09/15 
 Pct Recovery = 95%  Analysis Date = 08/06/15 
 Pct Recovery = 94%  Analysis Date = 08/06/15 
 Pct Recovery = 94%  Analysis Date = 08/02/15 
 Pct Recovery = 93%  Analysis Date = 08/02/15 
 Pct Recovery = 93%  Analysis Date = 07/30/15 
 Pct Recovery = 92%  Analysis Date = 07/30/15 
 Pct Recovery = 92%  Analysis Date = 07/27/15 
 Pct Recovery = 91%  Analysis Date = 07/27/15 
 Pct Recovery = 91%  Analysis Date = 07/24/15 
 Pct Recovery = 89%  Analysis Date = 07/24/15 
 Pct Recovery = 89%  Analysis Date = 07/20/15 
 Pct Recovery = 87%  Analysis Date = 07/20/15 
 Pct Recovery = 87%  Analysis Date = 07/17/15 
 Pct Recovery = 86%  Analysis Date = 07/17/15 
 Pct Recovery = 86%  Analysis Date = 07/14/15 
 Pct Recovery = 84%  Analysis Date = 07/14/15 
 Pct Recovery = 84%  Analysis Date = 07/10/15 
 Pct Recovery = 82%  Analysis Date = 07/10/15 
 Pct Recovery = 82%  Analysis Date = 07/07/15 
 Pct Recovery = 81%  Analysis Date = 07/07/15 
 Pct Recovery = 81%  Analysis Date = 07/04/15 
 Pct Recovery = 79%  Analysis Date = 07/04/15 
 Pct Recovery = 79%  Analysis Date = 07/01/15 
 Pct Recovery = 77%  Analysis Date = 07/01/15 
 Pct Recovery = 77%  Analysis Date = 06/27/15 
 Pct Recovery = 76%  Analysis Date = 06/27/15 
 Pct Recovery = 76%  Analysis Date = 06/24/15 
 Pct Recovery = 74%  Analysis Date = 06/24/15 
 Pct Recovery = 74%  Analysis Date = 06/21/15 
 Pct Recovery = 72%  Analysis Date = 06/21/15 
 Pct Recovery = 72%  Analysis Date = 06/18/15 
 Pct Recovery = 71%  Analysis Date = 06/18/15 
 Pct Recovery = 71%  Analysis Date = 06/14/15 
 Pct Recovery = 69%  Analysis Date = 06/14/15 
 Pct Recovery = 69%  Analysis Date = 06/11/15 
 Pct Recovery = 67%  Analysis Date = 06/11/15 
 Pct Recovery = 67%  Analysis Date = 06/08/15 
 Pct Recovery = 65%  Analysis Date = 06/08/15 
 Pct Recovery = 65%  Analysis Date = 06/04/15 
 Pct Recovery = 64%  Analysis Date = 06/04/15 
 Pct Recovery = 64%  Analysis Date = 06/01/15 
 Pct Recovery = 62%  Analysis Date = 06/01/15 
 Pct Recovery = 62%  Analysis Date = 05/29/15 
 Pct Recovery = 60%  Analysis Date = 05/29/15 
 Pct Recovery = 60%  Analysis Date = 05/26/15 
 Pct Recovery = 58%  Analysis Date = 05/26/15 
 Pct Recovery = 58%  Analysis Date = 05/22/15 
 Pct Recovery = 57%  Analysis Date = 05/22/15 
 Pct Recovery = 57%  Analysis Date = 05/19/15 
 Pct Recovery = 55%  Analysis Date = 05/19/15 
 Pct Recovery = 55%  Analysis Date = 05/16/15 
 Pct Recovery = 53%  Analysis Date = 05/16/15 
 Pct Recovery = 53%  Analysis Date = 05/13/15 
 Pct Recovery = 52%  Analysis Date = 05/13/15 
 Pct Recovery = 52%  Analysis Date = 05/09/15 
 Pct Recovery = 50%  Analysis Date = 05/09/15 
 Pct Recovery = 50%  Analysis Date = 05/06/15 
 Pct Recovery = 48%  Analysis Date = 05/06/15 
 Pct Recovery = 48%  Analysis Date = 05/03/15 
 Pct Recovery = 46%  Analysis Date = 05/03/15 
 Pct Recovery = 46%  Analysis Date = 04/30/15 
 Pct Recovery = 45%  Analysis Date = 04/30/15 
 Pct Recovery = 45%  Analysis Date = 04/26/15 
 Pct Recovery = 43%  Analysis Date = 04/26/15 
 Pct Recovery = 43%  Analysis Date = 04/23/15 
 Pct Recovery = 41%  Analysis Date = 04/23/15 
 Pct Recovery = 41%  Analysis Date = 04/20/15 
 Pct Recovery = 40%  Analysis Date = 04/20/15 
 Pct Recovery = 40%  Analysis Date = 04/16/15 
 Pct Recovery = 38%  Analysis Date = 04/16/15 
 Pct Recovery = 38%  Analysis Date = 04/13/15 
 Pct Recovery = 36%  Analysis Date = 04/13/15 
 Pct Recovery = 36%  Analysis Date = 04/10/15 
 Pct Recovery = 34%  Analysis Date = 04/10/15 
 Pct Recovery = 34%  Analysis Date = 04/07/15 
 Pct Recovery = 33%  Analysis Date = 04/07/15 
 Pct Recovery = 33%  Analysis Date = 04/03/15 
 Pct Recovery = 31%  Analysis Date = 04/03/15 
 Pct Recovery = 31%  Analysis Date = 03/31/15 
 Pct Recovery = 29%  Analysis Date = 03/31/15 
 Pct Recovery = 29%  Analysis Date = 03/28/15 
 Pct Recovery = 27%  Analysis Date = 03/28/15 
 Pct Recovery = 27%  Analysis Date = 03/25/15 
 Pct Recovery = 26%  Analysis Date = 03/25/15 
 Pct Recovery = 26%  Analysis Date = 03/21/15 
 Pct Recovery = 24%  Analysis Date = 03/21/15 
 Pct Recovery = 24%  Analysis Date = 03/18/15 
 Pct Recovery = 23%  Analysis Date = 03/18/15 
 Pct Recovery = 23%  Analysis Date = 03/15/15 
 Pct Recovery = 24%  Analysis Date = 03/15/15 
 Pct Recovery = 24%  Analysis Date = 03/11/15 
 Pct Recovery = 26%  Analysis Date = 03/11/15 
 Pct Recovery = 26%  Analysis Date = 03/08/15 
 Pct Recovery = 27%  Analysis Date = 03/08/15 
 Pct Recovery = 27%  Analysis Date = 03/05/15 
 Pct Recovery = 28%  Analysis Date = 03/05/15 
 Pct Recovery = 28%  Analysis Date = 03/02/15 
 Pct Recovery = 30%  Analysis Date = 03/02/15 
 Pct Recovery = 30%  Analysis Date = 02/26/15 
 Pct Recovery = 31%  Analysis Date = 02/26/15 
 Pct Recovery = 31%  Analysis Date = 02/23/15 
 Pct Recovery = 33%  Analysis Date = 02/23/15 
 Pct Recovery = 33%  Analysis Date = 02/20/15 
 Pct Recovery = 34%  Analysis Date = 02/20/15 
 Pct Recovery = 34%  Analysis Date = 02/17/15 
 Pct Recovery = 35%  Analysis Date = 02/17/15 
 Pct Recovery = 35%  Analysis Date = 02/13/15 
 Pct Recovery = 37%  Analysis Date = 02/13/15 
 Pct Recovery = 37%  Analysis Date = 02/10/15 
 Pct Recovery = 38%  Analysis Date = 02/10/15 
 Pct Recovery = 38%  Analysis Date = 02/07/15 
 Pct Recovery = 40%  Analysis Date = 02/07/15 
 Pct Recovery = 40%  Analysis Date = 02/03/15 
 Pct Recovery = 41%  Analysis Date = 02/03/15 
 Pct Recovery = 41%  Analysis Date = 01/31/15 
 Pct Recovery = 42%  Analysis Date = 01/31/15 
 Pct Recovery = 42%  Analysis Date = 01/28/15 
 Pct Recovery = 44%  Analysis Date = 01/28/15 
 Pct Recovery = 44%  Analysis Date = 01/25/15 
 Pct Recovery = 45%  Analysis Date = 01/25/15 
 Pct Recovery = 45%  Analysis Date = 01/21/15 
 Pct Recovery = 46%  Analysis Date = 01/21/15 
 Pct Recovery = 46%  Analysis Date = 01/18/15 
 Pct Recovery = 48%  Analysis Date = 01/18/15 
 Pct Recovery = 48%  Analysis Date = 01/15/15 
 Pct Recovery = 49%  Analysis Date = 01/15/15 
 Pct Recovery = 49%  Analysis Date = 01/12/15 
 Pct Recovery = 51%  Analysis Date = 01/12/15 
 Pct Recovery = 51%  Analysis Date = 01/08/15 
 Pct Recovery = 52%  Analysis Date = 01/08/15 
 Pct Recovery = 52%  Analysis Date = 01/05/15 
 Pct Recovery = 53%  Analysis Date = 01/05/15 
 Pct Recovery = 53%  Analysis Date = 01/02/15 
 Pct Recovery = 55%  Analysis Date = 01/02/15 
 Pct Recovery = 55%  Analysis Date = 12/30/14 
 Pct Recovery = 56%  Analysis Date = 12/30/14 
 Pct Recovery = 56%  Analysis Date = 12/26/14 
 Pct Recovery = 58%  Analysis Date = 12/26/14 
 Pct Recovery = 58%  Analysis Date = 12/23/14 
 Pct Recovery = 59%  Analysis Date = 12/23/14 
 Pct Recovery = 59%  Analysis Date = 12/20/14 
 Pct Recovery = 60%  Analysis Date = 12/20/14 
 Pct Recovery = 60%  Analysis Date = 12/16/14 
 Pct Recovery = 62%  Analysis Date = 12/16/14 
 Pct Recovery = 62%  Analysis Date = 12/13/14 
 Pct Recovery = 63%  Analysis Date = 12/13/14 
 Pct Recovery = 63%  Analysis Date = 12/10/14 
 Pct Recovery = 65%  Analysis Date = 12/10/14 
 Pct Recovery = 65%  Analysis Date = 12/07/14 
 Pct Recovery = 66%  Analysis Date = 12/07/14 
 Pct Recovery = 66%  Analysis Date = 12/03/14 
 Pct Recovery = 67%  Analysis Date = 12/03/14 
 Pct Recovery = 67%  Analysis Date = 11/30/14 
 Pct Recovery = 69%  Analysis Date = 11/30/14 
 Pct Recovery = 69%  Analysis Date = 11/27/14 
 Pct Recovery = 70%  Analysis Date = 11/27/14 
 Pct Recovery = 70%  Analysis Date = 11/24/14 
 Pct Recovery = 72%  Analysis Date = 11/24/14 
 Pct Recovery = 72%  Analysis Date = 11/20/14 
 Pct Recovery = 73%  Analysis Date = 11/20/14 
 Pct Recovery = 73%  Analysis Date = 11/17/14 
 Pct Recovery = 74%  Analysis Date = 11/17/14 
 Pct Recovery = 74%  Analysis Date = 11/14/14 
 Pct Recovery = 76%  Analysis Date = 11/14/14 
 Pct Recovery = 76%  Analysis Date = 11/10/14 
 Pct Recovery = 77%  Analysis Date = 11/10/14 
 Pct Recovery = 77%  Analysis Date = 11/07/14 
 Pct Recovery = 79%  Analysis Date = 11/07/14 
 Pct Recovery = 79%  Analysis Date = 11/04/14 
 Pct Recovery = 80%  Analysis Date = 11/04/14 
 Pct Recovery = 80%  Analysis Date = 11/01/14 
 Pct Recovery = 81%  Analysis Date = 11/01/14 
 Pct Recovery = 81%  Analysis Date = 10/28/14 
 Pct Recovery = 83%  Analysis Date = 10/28/14 
 Pct Recovery = 83%  Analysis Date = 10/25/14 
 Pct Recovery = 84%  Analysis Date = 10/25/14 
 Pct Recovery = 84%  Analysis Date = 10/22/14 
 Pct Recovery = 86%  Analysis Date = 10/22/14 
 Pct Recovery = 86%  Analysis Date = 10/19/14 
 Pct Recovery = 87%  Analysis Date = 10/19/14 
 Pct Recovery = 87%  Analysis Date = 10/15/14 
 Pct Recovery = 88%  Analysis Date = 10/15/14 
 Pct Recovery = 88%  Analysis Date = 10/12/14 
 Pct Recovery = 90%  Analysis Date = 10/12/14 
 Pct Recovery = 90%  Analysis Date = 10/09/14 
 Pct Recovery = 91%  Analysis Date = 10/09/14 
 Pct Recovery = 91%  Analysis Date = 10/05/14 
 Pct Recovery = 93%  Analysis Date = 10/05/14 
 Pct Recovery = 93%  Analysis Date = 10/02/14 
 Pct Recovery = 94%  Analysis Date = 10/02/14 
 Pct Recovery = 94%  Analysis Date = 09/29/14 
 Pct Recovery = 95%  Analysis Date = 09/29/14 
 Pct Recovery = 95%  Analysis Date = 09/26/14 
 Pct Recovery = 97%  Analysis Date = 09/26/14 
 Pct Recovery = 97%  Analysis Date = 09/22/14 
 Pct Recovery = 98%  Analysis Date = 09/22/14 
 Pct Recovery = 98%  Analysis Date = 09/19/14 
 Pct Recovery = 100%  Analysis Date = 09/19/14 
 Pct Recovery = 100%  Analysis Date = 09/16/14 
 Pct Recovery = 101%  Analysis Date = 09/16/14 
 Pct Recovery = 101%  Analysis Date = 09/13/14 
 Pct Recovery = 102%  Analysis Date = 09/13/14 
 Pct Recovery = 102%  Analysis Date = 09/09/14 
 Pct Recovery = 104%  Analysis Date = 09/09/14 
 Pct Recovery = 104%  Analysis Date = 09/06/14 
 Pct Recovery = 105%  Analysis Date = 09/06/14 
 Pct Recovery = 105%  Analysis Date = 09/03/14 
 Pct Recovery = 107%  Analysis Date = 09/03/14 
 Pct Recovery = 107%  Analysis Date = 08/31/14 
 Pct Recovery = 110%  Analysis Date = 08/31/14 
 Pct Recovery = 110%  Analysis Date = 08/27/14 
 Pct Recovery = 112%  Analysis Date = 08/27/14 
 Pct Recovery = 112%  Analysis Date = 08/24/14 
 Pct Recovery = 114%  Analysis Date = 08/24/14 
 Pct Recovery = 114%  Analysis Date = 08/21/14 
 Pct Recovery = 116%  Analysis Date = 08/21/14 
 Pct Recovery = 116%  Analysis Date = 08/17/14 
 Pct Recovery = 119%  Analysis Date = 08/17/14 
 Pct Recovery = 119%  Analysis Date = 08/14/14 
 Pct Recovery = 121%  Analysis Date = 08/14/14 
 Pct Recovery = 121%  Analysis Date = 08/11/14 
 Pct Recovery = 124%  Analysis Date = 08/11/14 
 Pct Recovery = 124%  Analysis Date = 08/08/14 
 Pct Recovery = 127%  Analysis Date = 08/08/14 
 Pct Recovery = 127%  Analysis Date = 08/04/14 
 Pct Recovery = 129%  Analysis Date = 08/04/14 
 Pct Recovery = 129%  Analysis Date = 08/01/14 
 Pct Recovery = 132%  Analysis Date = 08/01/14 
 Pct Recovery = 132%  Analysis Date = 07/29/14 
 Pct Recovery = 134%  Analysis Date = 07/29/14 
 Pct Recovery = 134%  Analysis Date = 07/26/14 
 Pct Recovery = 137%  Analysis Date = 07/26/14 
 Pct Recovery = 137%  Analysis Date = 07/22/14 
 Pct Recovery = 139%  Analysis Date = 07/22/14 
 Pct Recovery = 139%  Analysis Date = 07/19/14 
 Pct Recovery = 142%  Analysis Date = 07/19/14 
 Pct Recovery = 142%  Analysis Date = 07/16/14 
 Pct Recovery = 145%  Analysis Date = 07/16/14 
 Pct Recovery = 145%  Analysis Date = 07/12/14 
 Pct Recovery = 147%  Analysis Date = 07/12/14 
 Pct Recovery = 147%  Analysis Date = 07/09/14 
 Pct Recovery = 150%  Analysis Date = 07/09/14 
 Pct Recovery = 150%  Analysis Date = 07/06/14 
 Pct Recovery = 152%  Analysis Date = 07/06/14 
 Pct Recovery = 152%  Analysis Date = 07/03/14 
 Pct Recovery = 155%  Analysis Date = 07/03/14 
 Pct Recovery = 155%  Analysis Date = 06/29/14 
 Pct Recovery = 157%  Analysis Date = 06/29/14 
 Pct Recovery = 157%  Analysis Date = 06/26/14 
 Pct Recovery = 160%  Analysis Date = 06/26/14 
 Pct Recovery = 160%  Analysis Date = 06/23/14 
 Pct Recovery = 162%  Analysis Date = 06/23/14 
 Pct Recovery = 162%  Analysis Date = 06/20/14 
 Pct Recovery = 165%  Analysis Date = 06/20/14 
 Pct Recovery = 165%  Analysis Date = 06/16/14 
 Pct Recovery = 168%  Analysis Date = 06/16/14 
 Pct Recovery = 168%  Analysis Date = 06/13/14 
 Pct Recovery = 170%  Analysis Date = 06/13/14 
 Pct Recovery = 170%  Analysis Date = 06/10/14 
 Pct Recovery = 173%  Analysis Date = 06/10/14 
 Pct Recovery = 173%  Analysis Date = 06/07/14 
 Pct Recovery = 176%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
ACROLEIN

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 1 21% . 21% 0%
>= Reporting Level 12 108% 59% 97% 34%
Total 13 102% 61% 92% 34%

Sample Statistics
ACROLEIN

Characteristic N % % Basis
Plotted 13 93% Spiked
Estimated Values 13 93% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 1 7% Spiked
Spiked 14 .  
False Negatives 0 0% 0 out of 14
Not Spiked 26 .  
False Positives 0 0% 0 out of 26

BQS OBSP Determination:
ALPHA-TERPINEOL
METHOD: 4437 , TESTIDCODE: 68730GM016
Open Data Set

 Analysis Date = 07/29/16 
 SpikeMix = Supelco LC20145V: 40 µl & NSI 041516: 40 µl & NSI 041416HVOC: 40 µl 
 Pct Recovery = 73%  Analysis Date = 07/06/16 
 SpikeMix = Accu 216041354: 40 µl & NSI 041516: 40 µl & NSI 041416HVOC: 40 µl 
 Pct Recovery = 81%  Analysis Date = 08/11/16 
 SpikeMix = Phenova B20160303: 25 µl & Supelco LC20145V: 25 µl & NSI 041416HVOC: 25 µl 
 Pct Recovery = 67%  Analysis Date = 05/21/16 
 SpikeMix = Supelco LC20145V: 25 µl & NSI 041516: 25 µl & NSI 041416HVOC: 25 µl 
 Pct Recovery = 100%  Analysis Date = 06/26/15 
 SpikeMix = ChemService 3818700: 25 µl & Accu 215041338: 25 µl 
 Pct Recovery = 82%  Analysis Date = 06/25/15 
 SpikeMix = ChemService 3818700: 25 µl & NSI 050515HVOC: 25 µl 
 Pct Recovery = 79%  Analysis Date = 01/22/16 
 SpikeMix = NSI 050515HVOC: 25 µl & ERA 0601-15-05: 25 µl 
 Pct Recovery = 82%  Analysis Date = 10/09/15 
 SpikeMix = ERA 0601-15-05: 25 µl & Accu 215041338: 25 µl 
 Pct Recovery = 89%  Analysis Date = 01/10/15 
 SpikeMix = Abs 032014: 20 µl & ERA 0321-14-05A: 20 µl 
 Pct Recovery = 95%  Analysis Date = 08/13/14 
 SpikeMix = ERA 0321-14-05: 20 µl & Accu 214031128: 20 µl 
 Pct Recovery = 126%  Analysis Date = 07/11/14 
 SpikeMix = ChemService 2615700: 20 µl & Accu 214031128: 20 µl 
 Pct Recovery = 101%  Analysis Date = 07/03/14 
 SpikeMix = Abs 032014: 20 µl & ChemService 2615700: 20 µl 
 Pct Recovery = 116%  Analysis Date = 06/07/14 
 SpikeMix = ChemService 2615700: 20 µl & Supelco LC06437: 20 µl 
 Pct Recovery = 103%  Analysis Date = 06/06/14 
 SpikeMix = NSI 031814: 20 µl & ChemService 2615700: 20 µl 
 Pct Recovery = 99%  Analysis Date = 07/27/16 
 SpikeMix = ChemService 5082800: 15 µl & Supelco LC20145V: 15 µl & Accu 216041225: 15 µl 
 Pct Recovery = 68%  Analysis Date = 08/12/16 
 SpikeMix = Accu 216041354: 15 µl & Abs 060916HVOC: 15 µl 
 Pct Recovery = 69%  Analysis Date = 07/06/16 
 SpikeMix = Phenova B20160303: 15 µl & Accu 216041354: 15 µl & NSI 041416HVOC: 15 µl 
 Pct Recovery = 65%  Analysis Date = 06/23/16 
 SpikeMix = . 
 Pct Recovery = 43%  Analysis Date = 05/20/16 
 SpikeMix = Accu 216041354: 15 µl & NSI 041516: 15 µl & Accu 216041225: 15 µl 
 Pct Recovery = 85%  Analysis Date = 04/28/16 
 SpikeMix = ChemService 3818700: 15 µl & Supelco LC13544: 15 µl 
 Pct Recovery = 101%  Analysis Date = 06/16/15 
 SpikeMix = ChemService 3818700: 15 µl & NSI 050515HVOC: 15 µl 
 Pct Recovery = 76%  Analysis Date = 05/14/15 
 SpikeMix = ChemService 3818700: 15 µl & Supelco LC13544: 15 µl 
 Pct Recovery = 100%  Analysis Date = 09/24/15 
 SpikeMix = Abs 040315: 15 µl & ERA 0601-15-05: 15 µl 
 Pct Recovery = 81%  Analysis Date = 08/24/15 
 SpikeMix = ERA 0601-15-05: 15 µl & Supelco LC13544: 15 µl 
 Pct Recovery = 88%  Analysis Date = 04/25/15 
 SpikeMix = Abs 032014: 10 µl & ERA 0321-14-05A: 10 µl 
 Pct Recovery = 92%  Analysis Date = 11/13/14 
 SpikeMix = ERA 0321-14-05A: 10 µl & Accu 214031128: 10 µl 
 Pct Recovery = 81%  Analysis Date = 09/06/14 
 SpikeMix = ERA 0321-14-05: 10 µl & Supelco LC06437: 10 µl 
 Pct Recovery = 139%  Analysis Date = 11/22/14 
 SpikeMix = ChemService 2615700: 10 µl & Supelco LC06437: 10 µl 
 Pct Recovery = 92%  Analysis Date = 07/30/14 
 SpikeMix = NSI 031814: 10 µl & ChemService 2615700: 10 µl 
 Pct Recovery = 138%  Analysis Date = 05/20/14 
 SpikeMix = ChemService 2615700: 10 µl & Accu 214031128: 10 µl 
 Pct Recovery = 123%  Analysis Date = 04/09/16 
 SpikeMix = Abs 040315: 10 µl & ChemService 3818700: 10 µl 
 Pct Recovery = 71%  Analysis Date = 12/10/15 
 SpikeMix = ChemService 3818700: 10 µl & Supelco LC13544: 10 µl 
 Pct Recovery = 69%  Analysis Date = 10/23/15 
 SpikeMix = Abs 040315: 10 µl & ChemService 3818700: 10 µl 
 Pct Recovery = 92%  Analysis Date = 05/20/15 
 SpikeMix = ChemService 3818700: 10 µl & Accu 215041338: 10 µl 
 Pct Recovery = 110%  Analysis Date = 02/12/16 
 SpikeMix = ERA 0601-15-05: 10 µl & Accu 215041338: 10 µl 
 Pct Recovery = 74%  Analysis Date = 12/05/15 
 SpikeMix = NSI 050515HVOC: 10 µl & ERA 0601-15-05: 10 µl 
 Pct Recovery = 71%  Analysis Date = 11/14/15 
 SpikeMix = ERA 0601-15-05: 10 µl 
 Pct Recovery = 80%  Analysis Date = 08/14/15 
 SpikeMix = Abs 040315: 10 µl & ERA 0601-15-05: 10 µl 
 Pct Recovery = 61%  Analysis Date = 08/12/16 
 Pct Recovery = 71%  Analysis Date = 08/07/16 
 Pct Recovery = 72%  Analysis Date = 08/07/16 
 Pct Recovery = 72%  Analysis Date = 08/03/16 
 Pct Recovery = 72%  Analysis Date = 08/03/16 
 Pct Recovery = 72%  Analysis Date = 07/30/16 
 Pct Recovery = 72%  Analysis Date = 07/30/16 
 Pct Recovery = 72%  Analysis Date = 07/26/16 
 Pct Recovery = 72%  Analysis Date = 07/26/16 
 Pct Recovery = 72%  Analysis Date = 07/22/16 
 Pct Recovery = 72%  Analysis Date = 07/22/16 
 Pct Recovery = 72%  Analysis Date = 07/18/16 
 Pct Recovery = 72%  Analysis Date = 07/18/16 
 Pct Recovery = 72%  Analysis Date = 07/14/16 
 Pct Recovery = 73%  Analysis Date = 07/14/16 
 Pct Recovery = 73%  Analysis Date = 07/10/16 
 Pct Recovery = 73%  Analysis Date = 07/10/16 
 Pct Recovery = 73%  Analysis Date = 07/06/16 
 Pct Recovery = 73%  Analysis Date = 07/06/16 
 Pct Recovery = 73%  Analysis Date = 07/02/16 
 Pct Recovery = 73%  Analysis Date = 07/02/16 
 Pct Recovery = 73%  Analysis Date = 06/28/16 
 Pct Recovery = 73%  Analysis Date = 06/28/16 
 Pct Recovery = 73%  Analysis Date = 06/24/16 
 Pct Recovery = 73%  Analysis Date = 06/24/16 
 Pct Recovery = 73%  Analysis Date = 06/20/16 
 Pct Recovery = 74%  Analysis Date = 06/20/16 
 Pct Recovery = 74%  Analysis Date = 06/15/16 
 Pct Recovery = 74%  Analysis Date = 06/15/16 
 Pct Recovery = 74%  Analysis Date = 06/11/16 
 Pct Recovery = 74%  Analysis Date = 06/11/16 
 Pct Recovery = 74%  Analysis Date = 06/07/16 
 Pct Recovery = 74%  Analysis Date = 06/07/16 
 Pct Recovery = 74%  Analysis Date = 06/03/16 
 Pct Recovery = 74%  Analysis Date = 06/03/16 
 Pct Recovery = 74%  Analysis Date = 05/30/16 
 Pct Recovery = 74%  Analysis Date = 05/30/16 
 Pct Recovery = 74%  Analysis Date = 05/26/16 
 Pct Recovery = 75%  Analysis Date = 05/26/16 
 Pct Recovery = 75%  Analysis Date = 05/22/16 
 Pct Recovery = 75%  Analysis Date = 05/22/16 
 Pct Recovery = 75%  Analysis Date = 05/18/16 
 Pct Recovery = 75%  Analysis Date = 05/18/16 
 Pct Recovery = 75%  Analysis Date = 05/14/16 
 Pct Recovery = 75%  Analysis Date = 05/14/16 
 Pct Recovery = 75%  Analysis Date = 05/10/16 
 Pct Recovery = 75%  Analysis Date = 05/10/16 
 Pct Recovery = 75%  Analysis Date = 05/06/16 
 Pct Recovery = 75%  Analysis Date = 05/06/16 
 Pct Recovery = 75%  Analysis Date = 05/02/16 
 Pct Recovery = 76%  Analysis Date = 05/02/16 
 Pct Recovery = 76%  Analysis Date = 04/28/16 
 Pct Recovery = 76%  Analysis Date = 04/28/16 
 Pct Recovery = 76%  Analysis Date = 04/23/16 
 Pct Recovery = 76%  Analysis Date = 04/23/16 
 Pct Recovery = 76%  Analysis Date = 04/19/16 
 Pct Recovery = 76%  Analysis Date = 04/19/16 
 Pct Recovery = 76%  Analysis Date = 04/15/16 
 Pct Recovery = 76%  Analysis Date = 04/15/16 
 Pct Recovery = 76%  Analysis Date = 04/11/16 
 Pct Recovery = 76%  Analysis Date = 04/11/16 
 Pct Recovery = 76%  Analysis Date = 04/07/16 
 Pct Recovery = 77%  Analysis Date = 04/07/16 
 Pct Recovery = 77%  Analysis Date = 04/03/16 
 Pct Recovery = 77%  Analysis Date = 04/03/16 
 Pct Recovery = 77%  Analysis Date = 03/30/16 
 Pct Recovery = 77%  Analysis Date = 03/30/16 
 Pct Recovery = 77%  Analysis Date = 03/26/16 
 Pct Recovery = 77%  Analysis Date = 03/26/16 
 Pct Recovery = 77%  Analysis Date = 03/22/16 
 Pct Recovery = 77%  Analysis Date = 03/22/16 
 Pct Recovery = 77%  Analysis Date = 03/18/16 
 Pct Recovery = 77%  Analysis Date = 03/18/16 
 Pct Recovery = 77%  Analysis Date = 03/14/16 
 Pct Recovery = 78%  Analysis Date = 03/14/16 
 Pct Recovery = 78%  Analysis Date = 03/10/16 
 Pct Recovery = 78%  Analysis Date = 03/10/16 
 Pct Recovery = 78%  Analysis Date = 03/06/16 
 Pct Recovery = 78%  Analysis Date = 03/06/16 
 Pct Recovery = 78%  Analysis Date = 03/02/16 
 Pct Recovery = 78%  Analysis Date = 03/02/16 
 Pct Recovery = 78%  Analysis Date = 02/26/16 
 Pct Recovery = 78%  Analysis Date = 02/26/16 
 Pct Recovery = 78%  Analysis Date = 02/22/16 
 Pct Recovery = 78%  Analysis Date = 02/22/16 
 Pct Recovery = 78%  Analysis Date = 02/18/16 
 Pct Recovery = 79%  Analysis Date = 02/18/16 
 Pct Recovery = 79%  Analysis Date = 02/14/16 
 Pct Recovery = 79%  Analysis Date = 02/14/16 
 Pct Recovery = 79%  Analysis Date = 02/10/16 
 Pct Recovery = 79%  Analysis Date = 02/10/16 
 Pct Recovery = 79%  Analysis Date = 02/06/16 
 Pct Recovery = 79%  Analysis Date = 02/06/16 
 Pct Recovery = 79%  Analysis Date = 02/02/16 
 Pct Recovery = 79%  Analysis Date = 02/02/16 
 Pct Recovery = 79%  Analysis Date = 01/29/16 
 Pct Recovery = 79%  Analysis Date = 01/29/16 
 Pct Recovery = 79%  Analysis Date = 01/25/16 
 Pct Recovery = 79%  Analysis Date = 01/25/16 
 Pct Recovery = 79%  Analysis Date = 01/21/16 
 Pct Recovery = 79%  Analysis Date = 01/21/16 
 Pct Recovery = 79%  Analysis Date = 01/17/16 
 Pct Recovery = 79%  Analysis Date = 01/17/16 
 Pct Recovery = 79%  Analysis Date = 01/13/16 
 Pct Recovery = 79%  Analysis Date = 01/13/16 
 Pct Recovery = 79%  Analysis Date = 01/09/16 
 Pct Recovery = 79%  Analysis Date = 01/09/16 
 Pct Recovery = 79%  Analysis Date = 01/04/16 
 Pct Recovery = 79%  Analysis Date = 01/04/16 
 Pct Recovery = 79%  Analysis Date = 12/31/15 
 Pct Recovery = 79%  Analysis Date = 12/31/15 
 Pct Recovery = 79%  Analysis Date = 12/27/15 
 Pct Recovery = 79%  Analysis Date = 12/27/15 
 Pct Recovery = 79%  Analysis Date = 12/23/15 
 Pct Recovery = 79%  Analysis Date = 12/23/15 
 Pct Recovery = 79%  Analysis Date = 12/19/15 
 Pct Recovery = 80%  Analysis Date = 12/19/15 
 Pct Recovery = 80%  Analysis Date = 12/15/15 
 Pct Recovery = 80%  Analysis Date = 12/15/15 
 Pct Recovery = 80%  Analysis Date = 12/11/15 
 Pct Recovery = 80%  Analysis Date = 12/11/15 
 Pct Recovery = 80%  Analysis Date = 12/07/15 
 Pct Recovery = 80%  Analysis Date = 12/07/15 
 Pct Recovery = 80%  Analysis Date = 12/03/15 
 Pct Recovery = 80%  Analysis Date = 12/03/15 
 Pct Recovery = 80%  Analysis Date = 11/29/15 
 Pct Recovery = 80%  Analysis Date = 11/29/15 
 Pct Recovery = 80%  Analysis Date = 11/25/15 
 Pct Recovery = 80%  Analysis Date = 11/25/15 
 Pct Recovery = 80%  Analysis Date = 11/21/15 
 Pct Recovery = 80%  Analysis Date = 11/21/15 
 Pct Recovery = 80%  Analysis Date = 11/17/15 
 Pct Recovery = 80%  Analysis Date = 11/17/15 
 Pct Recovery = 80%  Analysis Date = 11/12/15 
 Pct Recovery = 80%  Analysis Date = 11/12/15 
 Pct Recovery = 80%  Analysis Date = 11/08/15 
 Pct Recovery = 80%  Analysis Date = 11/08/15 
 Pct Recovery = 80%  Analysis Date = 11/04/15 
 Pct Recovery = 80%  Analysis Date = 11/04/15 
 Pct Recovery = 80%  Analysis Date = 10/31/15 
 Pct Recovery = 80%  Analysis Date = 10/31/15 
 Pct Recovery = 80%  Analysis Date = 10/27/15 
 Pct Recovery = 81%  Analysis Date = 10/27/15 
 Pct Recovery = 81%  Analysis Date = 10/23/15 
 Pct Recovery = 81%  Analysis Date = 10/23/15 
 Pct Recovery = 81%  Analysis Date = 10/19/15 
 Pct Recovery = 81%  Analysis Date = 10/19/15 
 Pct Recovery = 81%  Analysis Date = 10/15/15 
 Pct Recovery = 81%  Analysis Date = 10/15/15 
 Pct Recovery = 81%  Analysis Date = 10/11/15 
 Pct Recovery = 81%  Analysis Date = 10/11/15 
 Pct Recovery = 81%  Analysis Date = 10/07/15 
 Pct Recovery = 81%  Analysis Date = 10/07/15 
 Pct Recovery = 81%  Analysis Date = 10/03/15 
 Pct Recovery = 82%  Analysis Date = 10/03/15 
 Pct Recovery = 82%  Analysis Date = 09/29/15 
 Pct Recovery = 82%  Analysis Date = 09/29/15 
 Pct Recovery = 82%  Analysis Date = 09/25/15 
 Pct Recovery = 82%  Analysis Date = 09/25/15 
 Pct Recovery = 82%  Analysis Date = 09/21/15 
 Pct Recovery = 82%  Analysis Date = 09/21/15 
 Pct Recovery = 82%  Analysis Date = 09/16/15 
 Pct Recovery = 82%  Analysis Date = 09/16/15 
 Pct Recovery = 82%  Analysis Date = 09/12/15 
 Pct Recovery = 83%  Analysis Date = 09/12/15 
 Pct Recovery = 83%  Analysis Date = 09/08/15 
 Pct Recovery = 83%  Analysis Date = 09/08/15 
 Pct Recovery = 83%  Analysis Date = 09/04/15 
 Pct Recovery = 83%  Analysis Date = 09/04/15 
 Pct Recovery = 83%  Analysis Date = 08/31/15 
 Pct Recovery = 83%  Analysis Date = 08/31/15 
 Pct Recovery = 83%  Analysis Date = 08/27/15 
 Pct Recovery = 83%  Analysis Date = 08/27/15 
 Pct Recovery = 83%  Analysis Date = 08/23/15 
 Pct Recovery = 83%  Analysis Date = 08/23/15 
 Pct Recovery = 83%  Analysis Date = 08/19/15 
 Pct Recovery = 84%  Analysis Date = 08/19/15 
 Pct Recovery = 84%  Analysis Date = 08/15/15 
 Pct Recovery = 84%  Analysis Date = 08/15/15 
 Pct Recovery = 84%  Analysis Date = 08/11/15 
 Pct Recovery = 84%  Analysis Date = 08/11/15 
 Pct Recovery = 84%  Analysis Date = 08/07/15 
 Pct Recovery = 84%  Analysis Date = 08/07/15 
 Pct Recovery = 84%  Analysis Date = 08/03/15 
 Pct Recovery = 84%  Analysis Date = 08/03/15 
 Pct Recovery = 84%  Analysis Date = 07/30/15 
 Pct Recovery = 85%  Analysis Date = 07/30/15 
 Pct Recovery = 85%  Analysis Date = 07/25/15 
 Pct Recovery = 85%  Analysis Date = 07/25/15 
 Pct Recovery = 85%  Analysis Date = 07/21/15 
 Pct Recovery = 85%  Analysis Date = 07/21/15 
 Pct Recovery = 85%  Analysis Date = 07/17/15 
 Pct Recovery = 85%  Analysis Date = 07/17/15 
 Pct Recovery = 85%  Analysis Date = 07/13/15 
 Pct Recovery = 85%  Analysis Date = 07/13/15 
 Pct Recovery = 85%  Analysis Date = 07/09/15 
 Pct Recovery = 86%  Analysis Date = 07/09/15 
 Pct Recovery = 86%  Analysis Date = 07/05/15 
 Pct Recovery = 86%  Analysis Date = 07/05/15 
 Pct Recovery = 86%  Analysis Date = 07/01/15 
 Pct Recovery = 86%  Analysis Date = 07/01/15 
 Pct Recovery = 86%  Analysis Date = 06/27/15 
 Pct Recovery = 86%  Analysis Date = 06/27/15 
 Pct Recovery = 86%  Analysis Date = 06/23/15 
 Pct Recovery = 86%  Analysis Date = 06/23/15 
 Pct Recovery = 86%  Analysis Date = 06/19/15 
 Pct Recovery = 87%  Analysis Date = 06/19/15 
 Pct Recovery = 87%  Analysis Date = 06/15/15 
 Pct Recovery = 87%  Analysis Date = 06/15/15 
 Pct Recovery = 87%  Analysis Date = 06/11/15 
 Pct Recovery = 87%  Analysis Date = 06/11/15 
 Pct Recovery = 87%  Analysis Date = 06/07/15 
 Pct Recovery = 87%  Analysis Date = 06/07/15 
 Pct Recovery = 87%  Analysis Date = 06/02/15 
 Pct Recovery = 87%  Analysis Date = 06/02/15 
 Pct Recovery = 87%  Analysis Date = 05/29/15 
 Pct Recovery = 87%  Analysis Date = 05/29/15 
 Pct Recovery = 87%  Analysis Date = 05/25/15 
 Pct Recovery = 88%  Analysis Date = 05/25/15 
 Pct Recovery = 88%  Analysis Date = 05/21/15 
 Pct Recovery = 88%  Analysis Date = 05/21/15 
 Pct Recovery = 88%  Analysis Date = 05/17/15 
 Pct Recovery = 88%  Analysis Date = 05/17/15 
 Pct Recovery = 88%  Analysis Date = 05/13/15 
 Pct Recovery = 88%  Analysis Date = 05/13/15 
 Pct Recovery = 88%  Analysis Date = 05/09/15 
 Pct Recovery = 89%  Analysis Date = 05/09/15 
 Pct Recovery = 89%  Analysis Date = 05/05/15 
 Pct Recovery = 89%  Analysis Date = 05/05/15 
 Pct Recovery = 89%  Analysis Date = 05/01/15 
 Pct Recovery = 89%  Analysis Date = 05/01/15 
 Pct Recovery = 89%  Analysis Date = 04/27/15 
 Pct Recovery = 90%  Analysis Date = 04/27/15 
 Pct Recovery = 90%  Analysis Date = 04/23/15 
 Pct Recovery = 90%  Analysis Date = 04/23/15 
 Pct Recovery = 90%  Analysis Date = 04/19/15 
 Pct Recovery = 90%  Analysis Date = 04/19/15 
 Pct Recovery = 90%  Analysis Date = 04/15/15 
 Pct Recovery = 91%  Analysis Date = 04/15/15 
 Pct Recovery = 91%  Analysis Date = 04/11/15 
 Pct Recovery = 91%  Analysis Date = 04/11/15 
 Pct Recovery = 91%  Analysis Date = 04/06/15 
 Pct Recovery = 91%  Analysis Date = 04/06/15 
 Pct Recovery = 91%  Analysis Date = 04/02/15 
 Pct Recovery = 92%  Analysis Date = 04/02/15 
 Pct Recovery = 92%  Analysis Date = 03/29/15 
 Pct Recovery = 92%  Analysis Date = 03/29/15 
 Pct Recovery = 92%  Analysis Date = 03/25/15 
 Pct Recovery = 93%  Analysis Date = 03/25/15 
 Pct Recovery = 93%  Analysis Date = 03/21/15 
 Pct Recovery = 93%  Analysis Date = 03/21/15 
 Pct Recovery = 93%  Analysis Date = 03/17/15 
 Pct Recovery = 93%  Analysis Date = 03/17/15 
 Pct Recovery = 93%  Analysis Date = 03/13/15 
 Pct Recovery = 94%  Analysis Date = 03/13/15 
 Pct Recovery = 94%  Analysis Date = 03/09/15 
 Pct Recovery = 94%  Analysis Date = 03/09/15 
 Pct Recovery = 94%  Analysis Date = 03/05/15 
 Pct Recovery = 94%  Analysis Date = 03/05/15 
 Pct Recovery = 94%  Analysis Date = 03/01/15 
 Pct Recovery = 95%  Analysis Date = 03/01/15 
 Pct Recovery = 95%  Analysis Date = 02/25/15 
 Pct Recovery = 95%  Analysis Date = 02/25/15 
 Pct Recovery = 95%  Analysis Date = 02/21/15 
 Pct Recovery = 96%  Analysis Date = 02/21/15 
 Pct Recovery = 96%  Analysis Date = 02/17/15 
 Pct Recovery = 96%  Analysis Date = 02/17/15 
 Pct Recovery = 96%  Analysis Date = 02/12/15 
 Pct Recovery = 96%  Analysis Date = 02/12/15 
 Pct Recovery = 96%  Analysis Date = 02/08/15 
 Pct Recovery = 97%  Analysis Date = 02/08/15 
 Pct Recovery = 97%  Analysis Date = 02/04/15 
 Pct Recovery = 97%  Analysis Date = 02/04/15 
 Pct Recovery = 97%  Analysis Date = 01/31/15 
 Pct Recovery = 97%  Analysis Date = 01/31/15 
 Pct Recovery = 97%  Analysis Date = 01/27/15 
 Pct Recovery = 98%  Analysis Date = 01/27/15 
 Pct Recovery = 98%  Analysis Date = 01/23/15 
 Pct Recovery = 98%  Analysis Date = 01/23/15 
 Pct Recovery = 98%  Analysis Date = 01/19/15 
 Pct Recovery = 98%  Analysis Date = 01/19/15 
 Pct Recovery = 98%  Analysis Date = 01/15/15 
 Pct Recovery = 99%  Analysis Date = 01/15/15 
 Pct Recovery = 99%  Analysis Date = 01/11/15 
 Pct Recovery = 99%  Analysis Date = 01/11/15 
 Pct Recovery = 99%  Analysis Date = 01/07/15 
 Pct Recovery = 100%  Analysis Date = 01/07/15 
 Pct Recovery = 100%  Analysis Date = 01/03/15 
 Pct Recovery = 100%  Analysis Date = 01/03/15 
 Pct Recovery = 100%  Analysis Date = 12/30/14 
 Pct Recovery = 100%  Analysis Date = 12/30/14 
 Pct Recovery = 100%  Analysis Date = 12/26/14 
 Pct Recovery = 101%  Analysis Date = 12/26/14 
 Pct Recovery = 101%  Analysis Date = 12/21/14 
 Pct Recovery = 101%  Analysis Date = 12/21/14 
 Pct Recovery = 101%  Analysis Date = 12/17/14 
 Pct Recovery = 101%  Analysis Date = 12/17/14 
 Pct Recovery = 101%  Analysis Date = 12/13/14 
 Pct Recovery = 102%  Analysis Date = 12/13/14 
 Pct Recovery = 102%  Analysis Date = 12/09/14 
 Pct Recovery = 102%  Analysis Date = 12/09/14 
 Pct Recovery = 102%  Analysis Date = 12/05/14 
 Pct Recovery = 103%  Analysis Date = 12/05/14 
 Pct Recovery = 103%  Analysis Date = 12/01/14 
 Pct Recovery = 103%  Analysis Date = 12/01/14 
 Pct Recovery = 103%  Analysis Date = 11/27/14 
 Pct Recovery = 103%  Analysis Date = 11/27/14 
 Pct Recovery = 103%  Analysis Date = 11/23/14 
 Pct Recovery = 104%  Analysis Date = 11/23/14 
 Pct Recovery = 104%  Analysis Date = 11/19/14 
 Pct Recovery = 104%  Analysis Date = 11/19/14 
 Pct Recovery = 104%  Analysis Date = 11/15/14 
 Pct Recovery = 104%  Analysis Date = 11/15/14 
 Pct Recovery = 104%  Analysis Date = 11/11/14 
 Pct Recovery = 105%  Analysis Date = 11/11/14 
 Pct Recovery = 105%  Analysis Date = 11/07/14 
 Pct Recovery = 105%  Analysis Date = 11/07/14 
 Pct Recovery = 105%  Analysis Date = 11/03/14 
 Pct Recovery = 105%  Analysis Date = 11/03/14 
 Pct Recovery = 105%  Analysis Date = 10/30/14 
 Pct Recovery = 105%  Analysis Date = 10/30/14 
 Pct Recovery = 105%  Analysis Date = 10/25/14 
 Pct Recovery = 106%  Analysis Date = 10/25/14 
 Pct Recovery = 106%  Analysis Date = 10/21/14 
 Pct Recovery = 106%  Analysis Date = 10/21/14 
 Pct Recovery = 106%  Analysis Date = 10/17/14 
 Pct Recovery = 106%  Analysis Date = 10/17/14 
 Pct Recovery = 106%  Analysis Date = 10/13/14 
 Pct Recovery = 107%  Analysis Date = 10/13/14 
 Pct Recovery = 107%  Analysis Date = 10/09/14 
 Pct Recovery = 107%  Analysis Date = 10/09/14 
 Pct Recovery = 107%  Analysis Date = 10/05/14 
 Pct Recovery = 107%  Analysis Date = 10/05/14 
 Pct Recovery = 107%  Analysis Date = 10/01/14 
 Pct Recovery = 108%  Analysis Date = 10/01/14 
 Pct Recovery = 108%  Analysis Date = 09/27/14 
 Pct Recovery = 108%  Analysis Date = 09/27/14 
 Pct Recovery = 108%  Analysis Date = 09/23/14 
 Pct Recovery = 108%  Analysis Date = 09/23/14 
 Pct Recovery = 108%  Analysis Date = 09/19/14 
 Pct Recovery = 109%  Analysis Date = 09/19/14 
 Pct Recovery = 109%  Analysis Date = 09/15/14 
 Pct Recovery = 109%  Analysis Date = 09/15/14 
 Pct Recovery = 109%  Analysis Date = 09/11/14 
 Pct Recovery = 109%  Analysis Date = 09/11/14 
 Pct Recovery = 109%  Analysis Date = 09/07/14 
 Pct Recovery = 109%  Analysis Date = 09/07/14 
 Pct Recovery = 109%  Analysis Date = 09/02/14 
 Pct Recovery = 110%  Analysis Date = 09/02/14 
 Pct Recovery = 110%  Analysis Date = 08/29/14 
 Pct Recovery = 110%  Analysis Date = 08/29/14 
 Pct Recovery = 110%  Analysis Date = 08/25/14 
 Pct Recovery = 110%  Analysis Date = 08/25/14 
 Pct Recovery = 110%  Analysis Date = 08/21/14 
 Pct Recovery = 111%  Analysis Date = 08/21/14 
 Pct Recovery = 111%  Analysis Date = 08/17/14 
 Pct Recovery = 111%  Analysis Date = 08/17/14 
 Pct Recovery = 111%  Analysis Date = 08/13/14 
 Pct Recovery = 111%  Analysis Date = 08/13/14 
 Pct Recovery = 111%  Analysis Date = 08/09/14 
 Pct Recovery = 112%  Analysis Date = 08/09/14 
 Pct Recovery = 112%  Analysis Date = 08/05/14 
 Pct Recovery = 112%  Analysis Date = 08/05/14 
 Pct Recovery = 112%  Analysis Date = 08/01/14 
 Pct Recovery = 112%  Analysis Date = 08/01/14 
 Pct Recovery = 112%  Analysis Date = 07/28/14 
 Pct Recovery = 113%  Analysis Date = 07/28/14 
 Pct Recovery = 113%  Analysis Date = 07/24/14 
 Pct Recovery = 113%  Analysis Date = 07/24/14 
 Pct Recovery = 113%  Analysis Date = 07/20/14 
 Pct Recovery = 113%  Analysis Date = 07/20/14 
 Pct Recovery = 113%  Analysis Date = 07/16/14 
 Pct Recovery = 114%  Analysis Date = 07/16/14 
 Pct Recovery = 114%  Analysis Date = 07/11/14 
 Pct Recovery = 114%  Analysis Date = 07/11/14 
 Pct Recovery = 114%  Analysis Date = 07/07/14 
 Pct Recovery = 114%  Analysis Date = 07/07/14 
 Pct Recovery = 114%  Analysis Date = 07/03/14 
 Pct Recovery = 115%  Analysis Date = 07/03/14 
 Pct Recovery = 115%  Analysis Date = 06/29/14 
 Pct Recovery = 115%  Analysis Date = 06/29/14 
 Pct Recovery = 115%  Analysis Date = 06/25/14 
 Pct Recovery = 115%  Analysis Date = 06/25/14 
 Pct Recovery = 115%  Analysis Date = 06/21/14 
 Pct Recovery = 116%  Analysis Date = 06/21/14 
 Pct Recovery = 116%  Analysis Date = 06/17/14 
 Pct Recovery = 116%  Analysis Date = 06/17/14 
 Pct Recovery = 116%  Analysis Date = 06/13/14 
 Pct Recovery = 116%  Analysis Date = 06/13/14 
 Pct Recovery = 116%  Analysis Date = 06/09/14 
 Pct Recovery = 117%  Analysis Date = 06/09/14 
 Pct Recovery = 117%  Analysis Date = 06/05/14 
 Pct Recovery = 117%  Analysis Date = 06/05/14 
 Pct Recovery = 117%  Analysis Date = 06/01/14 
 Pct Recovery = 117%  Analysis Date = 06/01/14 
 Pct Recovery = 117%  Analysis Date = 05/28/14 
 Pct Recovery = 117%  Analysis Date = 05/28/14 
 Pct Recovery = 117%  Analysis Date = 05/24/14 
 Pct Recovery = 118%  Analysis Date = 05/24/14 
 Pct Recovery = 118%  Analysis Date = 05/20/14 
 Pct Recovery = 118%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
ALPHA-TERPINEOL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 38 88% 21% 84% 20%
Total 38 88% 21% 84% 20%

Sample Statistics
ALPHA-TERPINEOL

Characteristic N % % Basis
Plotted 38 100% Spiked
Estimated Values 1 3% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 38 .  
False Negatives 0 0% 0 out of 38
Not Spiked 17 .  
False Positives 0 0% 0 out of 17

BQS OBSP Determination:
BUTANAL
METHOD: 4437 , TESTIDCODE: 68732GM016
Open Data Set

 Analysis Date = 03/19/15 
 SpikeMix = Supelco LC06437: 20 µl & NSI 031814: 20 µl 
 Pct Recovery = 99%  Analysis Date = 08/20/14 
 SpikeMix = Supelco LC06437: 20 µl & Abs 032014: 20 µl 
 Pct Recovery = 88%  Analysis Date = 06/07/14 
 SpikeMix = ChemService 2615700: 20 µl & Supelco LC06437: 20 µl 
 Pct Recovery = 93%  Analysis Date = 08/13/14 
 SpikeMix = ERA 0321-14-05: 20 µl & Accu 214031128: 20 µl 
 Pct Recovery = 93%  Analysis Date = 07/23/14 
 SpikeMix = Accu 214031128: 20 µl & Abs 032014: 20 µl 
 Pct Recovery = 85%  Analysis Date = 07/11/14 
 SpikeMix = ChemService 2615700: 20 µl & Accu 214031128: 20 µl 
 Pct Recovery = 101%  Analysis Date = 05/07/14 
 SpikeMix = NSI 031814: 20 µl & Accu 214031128: 20 µl 
 Pct Recovery = 91%  Analysis Date = 01/22/16 
 SpikeMix = NSI 050515HVOC: 25 µl & ERA 0601-15-05: 25 µl 
 Pct Recovery = 80%  Analysis Date = 10/09/15 
 SpikeMix = Supelco LC13544: 25 µl & NSI 050515HVOC: 25 µl 
 Pct Recovery = 85%  Analysis Date = 06/25/15 
 SpikeMix = ChemService 3818700: 25 µl & NSI 050515HVOC: 25 µl 
 Pct Recovery = 84%  Analysis Date = 08/12/16 
 SpikeMix = Accu 216041354: 15 µl & Abs 060916HVOC: 15 µl 
 Pct Recovery = 93%  Analysis Date = 11/25/15 
 SpikeMix = Accu 215041338: 15 µl & Abs 040315: 15 µl 
 Pct Recovery = 78%  Analysis Date = 09/24/15 
 SpikeMix = Abs 040315: 15 µl & ERA 0601-15-05: 15 µl 
 Pct Recovery = 86%  Analysis Date = 09/05/15 
 SpikeMix = Accu 215041338: 15 µl & NSI 050515HVOC: 15 µl 
 Pct Recovery = 82%  Analysis Date = 07/30/15 
 SpikeMix = Supelco LC13544: 15 µl & NSI 050515HVOC: 15 µl 
 Pct Recovery = 84%  Analysis Date = 06/16/15 
 SpikeMix = ChemService 3818700: 15 µl & NSI 050515HVOC: 15 µl 
 Pct Recovery = 93%  Analysis Date = 11/22/14 
 SpikeMix = ChemService 2615700: 10 µl & Supelco LC06437: 10 µl 
 Pct Recovery = 96%  Analysis Date = 09/06/14 
 SpikeMix = ERA 0321-14-05: 10 µl & Supelco LC06437: 10 µl 
 Pct Recovery = 108%  Analysis Date = 06/17/14 
 SpikeMix = Supelco LC06437: 10 µl & Abs 032014: 10 µl 
 Pct Recovery = 99%  Analysis Date = 12/13/14 
 SpikeMix = Accu 214031128: 10 µl & NSI 031814: 10 µl 
 Pct Recovery = 95%  Analysis Date = 10/21/14 
 SpikeMix = ERA 0321-14-05A: 10 µl & Accu 214031128: 10 µl 
 Pct Recovery = 87%  Analysis Date = 09/11/14 
 SpikeMix = Accu 214031128: 10 µl & Abs 032014: 10 µl 
 Pct Recovery = 100%  Analysis Date = 05/20/14 
 SpikeMix = ChemService 2615700: 10 µl & Accu 214031128: 10 µl 
 Pct Recovery = 85%  Analysis Date = 04/09/16 
 SpikeMix = Abs 040315: 10 µl & ChemService 3818700: 10 µl 
 Pct Recovery = 88%  Analysis Date = 01/05/16 
 SpikeMix = Accu 215041338: 10 µl & Abs 040315: 10 µl 
 Pct Recovery = 85%  Analysis Date = 10/23/15 
 SpikeMix = Abs 040315: 10 µl & ChemService 3818700: 10 µl 
 Pct Recovery = 87%  Analysis Date = 08/14/15 
 SpikeMix = Abs 040315: 10 µl & ERA 0601-15-05: 10 µl 
 Pct Recovery = 84%  Analysis Date = 05/05/15 
 SpikeMix = Supelco LC13544: 10 µl & Abs 040315: 10 µl 
 Pct Recovery = 96%  Analysis Date = 03/22/16 
 SpikeMix = Supelco LC13544: 10 µl & NSI 050515HVOC: 10 µl 
 Pct Recovery = 86%  Analysis Date = 12/05/15 
 SpikeMix = NSI 050515HVOC: 10 µl & ERA 0601-15-05: 10 µl 
 Pct Recovery = 82%  Analysis Date = 08/11/16 
 Pct Recovery = 88%  Analysis Date = 08/07/16 
 Pct Recovery = 88%  Analysis Date = 08/07/16 
 Pct Recovery = 88%  Analysis Date = 08/03/16 
 Pct Recovery = 88%  Analysis Date = 08/03/16 
 Pct Recovery = 88%  Analysis Date = 07/30/16 
 Pct Recovery = 87%  Analysis Date = 07/30/16 
 Pct Recovery = 87%  Analysis Date = 07/26/16 
 Pct Recovery = 87%  Analysis Date = 07/26/16 
 Pct Recovery = 87%  Analysis Date = 07/22/16 
 Pct Recovery = 87%  Analysis Date = 07/22/16 
 Pct Recovery = 87%  Analysis Date = 07/18/16 
 Pct Recovery = 87%  Analysis Date = 07/18/16 
 Pct Recovery = 87%  Analysis Date = 07/14/16 
 Pct Recovery = 87%  Analysis Date = 07/14/16 
 Pct Recovery = 87%  Analysis Date = 07/09/16 
 Pct Recovery = 87%  Analysis Date = 07/09/16 
 Pct Recovery = 87%  Analysis Date = 07/05/16 
 Pct Recovery = 87%  Analysis Date = 07/05/16 
 Pct Recovery = 87%  Analysis Date = 07/01/16 
 Pct Recovery = 87%  Analysis Date = 07/01/16 
 Pct Recovery = 87%  Analysis Date = 06/27/16 
 Pct Recovery = 87%  Analysis Date = 06/27/16 
 Pct Recovery = 87%  Analysis Date = 06/23/16 
 Pct Recovery = 87%  Analysis Date = 06/23/16 
 Pct Recovery = 87%  Analysis Date = 06/19/16 
 Pct Recovery = 87%  Analysis Date = 06/19/16 
 Pct Recovery = 87%  Analysis Date = 06/15/16 
 Pct Recovery = 87%  Analysis Date = 06/15/16 
 Pct Recovery = 87%  Analysis Date = 06/10/16 
 Pct Recovery = 87%  Analysis Date = 06/10/16 
 Pct Recovery = 87%  Analysis Date = 06/06/16 
 Pct Recovery = 87%  Analysis Date = 06/06/16 
 Pct Recovery = 87%  Analysis Date = 06/02/16 
 Pct Recovery = 87%  Analysis Date = 06/02/16 
 Pct Recovery = 87%  Analysis Date = 05/29/16 
 Pct Recovery = 87%  Analysis Date = 05/29/16 
 Pct Recovery = 87%  Analysis Date = 05/25/16 
 Pct Recovery = 87%  Analysis Date = 05/25/16 
 Pct Recovery = 87%  Analysis Date = 05/21/16 
 Pct Recovery = 87%  Analysis Date = 05/21/16 
 Pct Recovery = 87%  Analysis Date = 05/17/16 
 Pct Recovery = 87%  Analysis Date = 05/17/16 
 Pct Recovery = 87%  Analysis Date = 05/12/16 
 Pct Recovery = 86%  Analysis Date = 05/12/16 
 Pct Recovery = 86%  Analysis Date = 05/08/16 
 Pct Recovery = 86%  Analysis Date = 05/08/16 
 Pct Recovery = 86%  Analysis Date = 05/04/16 
 Pct Recovery = 86%  Analysis Date = 05/04/16 
 Pct Recovery = 86%  Analysis Date = 04/30/16 
 Pct Recovery = 86%  Analysis Date = 04/30/16 
 Pct Recovery = 86%  Analysis Date = 04/26/16 
 Pct Recovery = 86%  Analysis Date = 04/26/16 
 Pct Recovery = 86%  Analysis Date = 04/22/16 
 Pct Recovery = 86%  Analysis Date = 04/22/16 
 Pct Recovery = 86%  Analysis Date = 04/18/16 
 Pct Recovery = 86%  Analysis Date = 04/18/16 
 Pct Recovery = 86%  Analysis Date = 04/13/16 
 Pct Recovery = 86%  Analysis Date = 04/13/16 
 Pct Recovery = 86%  Analysis Date = 04/09/16 
 Pct Recovery = 86%  Analysis Date = 04/09/16 
 Pct Recovery = 86%  Analysis Date = 04/05/16 
 Pct Recovery = 86%  Analysis Date = 04/05/16 
 Pct Recovery = 86%  Analysis Date = 04/01/16 
 Pct Recovery = 86%  Analysis Date = 04/01/16 
 Pct Recovery = 86%  Analysis Date = 03/28/16 
 Pct Recovery = 86%  Analysis Date = 03/28/16 
 Pct Recovery = 86%  Analysis Date = 03/24/16 
 Pct Recovery = 86%  Analysis Date = 03/24/16 
 Pct Recovery = 86%  Analysis Date = 03/20/16 
 Pct Recovery = 86%  Analysis Date = 03/20/16 
 Pct Recovery = 86%  Analysis Date = 03/15/16 
 Pct Recovery = 86%  Analysis Date = 03/15/16 
 Pct Recovery = 86%  Analysis Date = 03/11/16 
 Pct Recovery = 86%  Analysis Date = 03/11/16 
 Pct Recovery = 86%  Analysis Date = 03/07/16 
 Pct Recovery = 86%  Analysis Date = 03/07/16 
 Pct Recovery = 86%  Analysis Date = 03/03/16 
 Pct Recovery = 86%  Analysis Date = 03/03/16 
 Pct Recovery = 86%  Analysis Date = 02/28/16 
 Pct Recovery = 86%  Analysis Date = 02/28/16 
 Pct Recovery = 86%  Analysis Date = 02/24/16 
 Pct Recovery = 86%  Analysis Date = 02/24/16 
 Pct Recovery = 86%  Analysis Date = 02/20/16 
 Pct Recovery = 85%  Analysis Date = 02/20/16 
 Pct Recovery = 85%  Analysis Date = 02/15/16 
 Pct Recovery = 85%  Analysis Date = 02/15/16 
 Pct Recovery = 85%  Analysis Date = 02/11/16 
 Pct Recovery = 85%  Analysis Date = 02/11/16 
 Pct Recovery = 85%  Analysis Date = 02/07/16 
 Pct Recovery = 85%  Analysis Date = 02/07/16 
 Pct Recovery = 85%  Analysis Date = 02/03/16 
 Pct Recovery = 85%  Analysis Date = 02/03/16 
 Pct Recovery = 85%  Analysis Date = 01/30/16 
 Pct Recovery = 85%  Analysis Date = 01/30/16 
 Pct Recovery = 85%  Analysis Date = 01/26/16 
 Pct Recovery = 85%  Analysis Date = 01/26/16 
 Pct Recovery = 85%  Analysis Date = 01/22/16 
 Pct Recovery = 85%  Analysis Date = 01/22/16 
 Pct Recovery = 85%  Analysis Date = 01/17/16 
 Pct Recovery = 85%  Analysis Date = 01/17/16 
 Pct Recovery = 85%  Analysis Date = 01/13/16 
 Pct Recovery = 85%  Analysis Date = 01/13/16 
 Pct Recovery = 85%  Analysis Date = 01/09/16 
 Pct Recovery = 85%  Analysis Date = 01/09/16 
 Pct Recovery = 85%  Analysis Date = 01/05/16 
 Pct Recovery = 85%  Analysis Date = 01/05/16 
 Pct Recovery = 85%  Analysis Date = 01/01/16 
 Pct Recovery = 85%  Analysis Date = 01/01/16 
 Pct Recovery = 85%  Analysis Date = 12/28/15 
 Pct Recovery = 85%  Analysis Date = 12/28/15 
 Pct Recovery = 85%  Analysis Date = 12/24/15 
 Pct Recovery = 85%  Analysis Date = 12/24/15 
 Pct Recovery = 85%  Analysis Date = 12/20/15 
 Pct Recovery = 85%  Analysis Date = 12/20/15 
 Pct Recovery = 85%  Analysis Date = 12/15/15 
 Pct Recovery = 85%  Analysis Date = 12/15/15 
 Pct Recovery = 85%  Analysis Date = 12/11/15 
 Pct Recovery = 85%  Analysis Date = 12/11/15 
 Pct Recovery = 85%  Analysis Date = 12/07/15 
 Pct Recovery = 85%  Analysis Date = 12/07/15 
 Pct Recovery = 85%  Analysis Date = 12/03/15 
 Pct Recovery = 85%  Analysis Date = 12/03/15 
 Pct Recovery = 85%  Analysis Date = 11/29/15 
 Pct Recovery = 85%  Analysis Date = 11/29/15 
 Pct Recovery = 85%  Analysis Date = 11/25/15 
 Pct Recovery = 85%  Analysis Date = 11/25/15 
 Pct Recovery = 85%  Analysis Date = 11/21/15 
 Pct Recovery = 85%  Analysis Date = 11/21/15 
 Pct Recovery = 85%  Analysis Date = 11/16/15 
 Pct Recovery = 85%  Analysis Date = 11/16/15 
 Pct Recovery = 85%  Analysis Date = 11/12/15 
 Pct Recovery = 85%  Analysis Date = 11/12/15 
 Pct Recovery = 85%  Analysis Date = 11/08/15 
 Pct Recovery = 85%  Analysis Date = 11/08/15 
 Pct Recovery = 85%  Analysis Date = 11/04/15 
 Pct Recovery = 85%  Analysis Date = 11/04/15 
 Pct Recovery = 85%  Analysis Date = 10/31/15 
 Pct Recovery = 85%  Analysis Date = 10/31/15 
 Pct Recovery = 85%  Analysis Date = 10/27/15 
 Pct Recovery = 85%  Analysis Date = 10/27/15 
 Pct Recovery = 85%  Analysis Date = 10/23/15 
 Pct Recovery = 85%  Analysis Date = 10/23/15 
 Pct Recovery = 85%  Analysis Date = 10/18/15 
 Pct Recovery = 85%  Analysis Date = 10/18/15 
 Pct Recovery = 85%  Analysis Date = 10/14/15 
 Pct Recovery = 85%  Analysis Date = 10/14/15 
 Pct Recovery = 85%  Analysis Date = 10/10/15 
 Pct Recovery = 85%  Analysis Date = 10/10/15 
 Pct Recovery = 85%  Analysis Date = 10/06/15 
 Pct Recovery = 85%  Analysis Date = 10/06/15 
 Pct Recovery = 85%  Analysis Date = 10/02/15 
 Pct Recovery = 85%  Analysis Date = 10/02/15 
 Pct Recovery = 85%  Analysis Date = 09/28/15 
 Pct Recovery = 86%  Analysis Date = 09/28/15 
 Pct Recovery = 86%  Analysis Date = 09/24/15 
 Pct Recovery = 86%  Analysis Date = 09/24/15 
 Pct Recovery = 86%  Analysis Date = 09/19/15 
 Pct Recovery = 86%  Analysis Date = 09/19/15 
 Pct Recovery = 86%  Analysis Date = 09/15/15 
 Pct Recovery = 86%  Analysis Date = 09/15/15 
 Pct Recovery = 86%  Analysis Date = 09/11/15 
 Pct Recovery = 86%  Analysis Date = 09/11/15 
 Pct Recovery = 86%  Analysis Date = 09/07/15 
 Pct Recovery = 86%  Analysis Date = 09/07/15 
 Pct Recovery = 86%  Analysis Date = 09/03/15 
 Pct Recovery = 86%  Analysis Date = 09/03/15 
 Pct Recovery = 86%  Analysis Date = 08/30/15 
 Pct Recovery = 86%  Analysis Date = 08/30/15 
 Pct Recovery = 86%  Analysis Date = 08/26/15 
 Pct Recovery = 87%  Analysis Date = 08/26/15 
 Pct Recovery = 87%  Analysis Date = 08/21/15 
 Pct Recovery = 87%  Analysis Date = 08/21/15 
 Pct Recovery = 87%  Analysis Date = 08/17/15 
 Pct Recovery = 87%  Analysis Date = 08/17/15 
 Pct Recovery = 87%  Analysis Date = 08/13/15 
 Pct Recovery = 87%  Analysis Date = 08/13/15 
 Pct Recovery = 87%  Analysis Date = 08/09/15 
 Pct Recovery = 87%  Analysis Date = 08/09/15 
 Pct Recovery = 87%  Analysis Date = 08/05/15 
 Pct Recovery = 87%  Analysis Date = 08/05/15 
 Pct Recovery = 87%  Analysis Date = 08/01/15 
 Pct Recovery = 88%  Analysis Date = 08/01/15 
 Pct Recovery = 88%  Analysis Date = 07/28/15 
 Pct Recovery = 88%  Analysis Date = 07/28/15 
 Pct Recovery = 88%  Analysis Date = 07/23/15 
 Pct Recovery = 88%  Analysis Date = 07/23/15 
 Pct Recovery = 88%  Analysis Date = 07/19/15 
 Pct Recovery = 88%  Analysis Date = 07/19/15 
 Pct Recovery = 88%  Analysis Date = 07/15/15 
 Pct Recovery = 88%  Analysis Date = 07/15/15 
 Pct Recovery = 88%  Analysis Date = 07/11/15 
 Pct Recovery = 89%  Analysis Date = 07/11/15 
 Pct Recovery = 89%  Analysis Date = 07/07/15 
 Pct Recovery = 89%  Analysis Date = 07/07/15 
 Pct Recovery = 89%  Analysis Date = 07/03/15 
 Pct Recovery = 89%  Analysis Date = 07/03/15 
 Pct Recovery = 89%  Analysis Date = 06/29/15 
 Pct Recovery = 89%  Analysis Date = 06/29/15 
 Pct Recovery = 89%  Analysis Date = 06/24/15 
 Pct Recovery = 89%  Analysis Date = 06/24/15 
 Pct Recovery = 89%  Analysis Date = 06/20/15 
 Pct Recovery = 90%  Analysis Date = 06/20/15 
 Pct Recovery = 90%  Analysis Date = 06/16/15 
 Pct Recovery = 90%  Analysis Date = 06/16/15 
 Pct Recovery = 90%  Analysis Date = 06/12/15 
 Pct Recovery = 90%  Analysis Date = 06/12/15 
 Pct Recovery = 90%  Analysis Date = 06/08/15 
 Pct Recovery = 90%  Analysis Date = 06/08/15 
 Pct Recovery = 90%  Analysis Date = 06/04/15 
 Pct Recovery = 90%  Analysis Date = 06/04/15 
 Pct Recovery = 90%  Analysis Date = 05/31/15 
 Pct Recovery = 90%  Analysis Date = 05/31/15 
 Pct Recovery = 90%  Analysis Date = 05/27/15 
 Pct Recovery = 91%  Analysis Date = 05/27/15 
 Pct Recovery = 91%  Analysis Date = 05/22/15 
 Pct Recovery = 91%  Analysis Date = 05/22/15 
 Pct Recovery = 91%  Analysis Date = 05/18/15 
 Pct Recovery = 91%  Analysis Date = 05/18/15 
 Pct Recovery = 91%  Analysis Date = 05/14/15 
 Pct Recovery = 91%  Analysis Date = 05/14/15 
 Pct Recovery = 91%  Analysis Date = 05/10/15 
 Pct Recovery = 91%  Analysis Date = 05/10/15 
 Pct Recovery = 91%  Analysis Date = 05/06/15 
 Pct Recovery = 91%  Analysis Date = 05/06/15 
 Pct Recovery = 91%  Analysis Date = 05/02/15 
 Pct Recovery = 92%  Analysis Date = 05/02/15 
 Pct Recovery = 92%  Analysis Date = 04/28/15 
 Pct Recovery = 92%  Analysis Date = 04/28/15 
 Pct Recovery = 92%  Analysis Date = 04/23/15 
 Pct Recovery = 92%  Analysis Date = 04/23/15 
 Pct Recovery = 92%  Analysis Date = 04/19/15 
 Pct Recovery = 92%  Analysis Date = 04/19/15 
 Pct Recovery = 92%  Analysis Date = 04/15/15 
 Pct Recovery = 92%  Analysis Date = 04/15/15 
 Pct Recovery = 92%  Analysis Date = 04/11/15 
 Pct Recovery = 92%  Analysis Date = 04/11/15 
 Pct Recovery = 92%  Analysis Date = 04/07/15 
 Pct Recovery = 92%  Analysis Date = 04/07/15 
 Pct Recovery = 92%  Analysis Date = 04/03/15 
 Pct Recovery = 92%  Analysis Date = 04/03/15 
 Pct Recovery = 92%  Analysis Date = 03/30/15 
 Pct Recovery = 92%  Analysis Date = 03/30/15 
 Pct Recovery = 92%  Analysis Date = 03/25/15 
 Pct Recovery = 92%  Analysis Date = 03/25/15 
 Pct Recovery = 92%  Analysis Date = 03/21/15 
 Pct Recovery = 93%  Analysis Date = 03/21/15 
 Pct Recovery = 93%  Analysis Date = 03/17/15 
 Pct Recovery = 93%  Analysis Date = 03/17/15 
 Pct Recovery = 93%  Analysis Date = 03/13/15 
 Pct Recovery = 93%  Analysis Date = 03/13/15 
 Pct Recovery = 93%  Analysis Date = 03/09/15 
 Pct Recovery = 93%  Analysis Date = 03/09/15 
 Pct Recovery = 93%  Analysis Date = 03/05/15 
 Pct Recovery = 93%  Analysis Date = 03/05/15 
 Pct Recovery = 93%  Analysis Date = 03/01/15 
 Pct Recovery = 93%  Analysis Date = 03/01/15 
 Pct Recovery = 93%  Analysis Date = 02/24/15 
 Pct Recovery = 93%  Analysis Date = 02/24/15 
 Pct Recovery = 93%  Analysis Date = 02/20/15 
 Pct Recovery = 93%  Analysis Date = 02/20/15 
 Pct Recovery = 93%  Analysis Date = 02/16/15 
 Pct Recovery = 93%  Analysis Date = 02/16/15 
 Pct Recovery = 93%  Analysis Date = 02/12/15 
 Pct Recovery = 93%  Analysis Date = 02/12/15 
 Pct Recovery = 93%  Analysis Date = 02/08/15 
 Pct Recovery = 94%  Analysis Date = 02/08/15 
 Pct Recovery = 94%  Analysis Date = 02/04/15 
 Pct Recovery = 94%  Analysis Date = 02/04/15 
 Pct Recovery = 94%  Analysis Date = 01/31/15 
 Pct Recovery = 94%  Analysis Date = 01/31/15 
 Pct Recovery = 94%  Analysis Date = 01/26/15 
 Pct Recovery = 94%  Analysis Date = 01/26/15 
 Pct Recovery = 94%  Analysis Date = 01/22/15 
 Pct Recovery = 94%  Analysis Date = 01/22/15 
 Pct Recovery = 94%  Analysis Date = 01/18/15 
 Pct Recovery = 94%  Analysis Date = 01/18/15 
 Pct Recovery = 94%  Analysis Date = 01/14/15 
 Pct Recovery = 94%  Analysis Date = 01/14/15 
 Pct Recovery = 94%  Analysis Date = 01/10/15 
 Pct Recovery = 94%  Analysis Date = 01/10/15 
 Pct Recovery = 94%  Analysis Date = 01/06/15 
 Pct Recovery = 94%  Analysis Date = 01/06/15 
 Pct Recovery = 94%  Analysis Date = 01/02/15 
 Pct Recovery = 94%  Analysis Date = 01/02/15 
 Pct Recovery = 94%  Analysis Date = 12/28/14 
 Pct Recovery = 95%  Analysis Date = 12/28/14 
 Pct Recovery = 95%  Analysis Date = 12/24/14 
 Pct Recovery = 95%  Analysis Date = 12/24/14 
 Pct Recovery = 95%  Analysis Date = 12/20/14 
 Pct Recovery = 95%  Analysis Date = 12/20/14 
 Pct Recovery = 95%  Analysis Date = 12/16/14 
 Pct Recovery = 95%  Analysis Date = 12/16/14 
 Pct Recovery = 95%  Analysis Date = 12/12/14 
 Pct Recovery = 95%  Analysis Date = 12/12/14 
 Pct Recovery = 95%  Analysis Date = 12/08/14 
 Pct Recovery = 95%  Analysis Date = 12/08/14 
 Pct Recovery = 95%  Analysis Date = 12/04/14 
 Pct Recovery = 95%  Analysis Date = 12/04/14 
 Pct Recovery = 95%  Analysis Date = 11/29/14 
 Pct Recovery = 95%  Analysis Date = 11/29/14 
 Pct Recovery = 95%  Analysis Date = 11/25/14 
 Pct Recovery = 95%  Analysis Date = 11/25/14 
 Pct Recovery = 95%  Analysis Date = 11/21/14 
 Pct Recovery = 95%  Analysis Date = 11/21/14 
 Pct Recovery = 95%  Analysis Date = 11/17/14 
 Pct Recovery = 95%  Analysis Date = 11/17/14 
 Pct Recovery = 95%  Analysis Date = 11/13/14 
 Pct Recovery = 95%  Analysis Date = 11/13/14 
 Pct Recovery = 95%  Analysis Date = 11/09/14 
 Pct Recovery = 95%  Analysis Date = 11/09/14 
 Pct Recovery = 95%  Analysis Date = 11/05/14 
 Pct Recovery = 95%  Analysis Date = 11/05/14 
 Pct Recovery = 95%  Analysis Date = 11/01/14 
 Pct Recovery = 95%  Analysis Date = 11/01/14 
 Pct Recovery = 95%  Analysis Date = 10/27/14 
 Pct Recovery = 95%  Analysis Date = 10/27/14 
 Pct Recovery = 95%  Analysis Date = 10/23/14 
 Pct Recovery = 95%  Analysis Date = 10/23/14 
 Pct Recovery = 95%  Analysis Date = 10/19/14 
 Pct Recovery = 95%  Analysis Date = 10/19/14 
 Pct Recovery = 95%  Analysis Date = 10/15/14 
 Pct Recovery = 95%  Analysis Date = 10/15/14 
 Pct Recovery = 95%  Analysis Date = 10/11/14 
 Pct Recovery = 95%  Analysis Date = 10/11/14 
 Pct Recovery = 95%  Analysis Date = 10/07/14 
 Pct Recovery = 95%  Analysis Date = 10/07/14 
 Pct Recovery = 95%  Analysis Date = 10/03/14 
 Pct Recovery = 95%  Analysis Date = 10/03/14 
 Pct Recovery = 95%  Analysis Date = 09/28/14 
 Pct Recovery = 95%  Analysis Date = 09/28/14 
 Pct Recovery = 95%  Analysis Date = 09/24/14 
 Pct Recovery = 95%  Analysis Date = 09/24/14 
 Pct Recovery = 95%  Analysis Date = 09/20/14 
 Pct Recovery = 95%  Analysis Date = 09/20/14 
 Pct Recovery = 95%  Analysis Date = 09/16/14 
 Pct Recovery = 95%  Analysis Date = 09/16/14 
 Pct Recovery = 95%  Analysis Date = 09/12/14 
 Pct Recovery = 94%  Analysis Date = 09/12/14 
 Pct Recovery = 94%  Analysis Date = 09/08/14 
 Pct Recovery = 94%  Analysis Date = 09/08/14 
 Pct Recovery = 94%  Analysis Date = 09/04/14 
 Pct Recovery = 94%  Analysis Date = 09/04/14 
 Pct Recovery = 94%  Analysis Date = 08/30/14 
 Pct Recovery = 94%  Analysis Date = 08/30/14 
 Pct Recovery = 94%  Analysis Date = 08/26/14 
 Pct Recovery = 94%  Analysis Date = 08/26/14 
 Pct Recovery = 94%  Analysis Date = 08/22/14 
 Pct Recovery = 94%  Analysis Date = 08/22/14 
 Pct Recovery = 94%  Analysis Date = 08/18/14 
 Pct Recovery = 94%  Analysis Date = 08/18/14 
 Pct Recovery = 94%  Analysis Date = 08/14/14 
 Pct Recovery = 94%  Analysis Date = 08/14/14 
 Pct Recovery = 94%  Analysis Date = 08/10/14 
 Pct Recovery = 94%  Analysis Date = 08/10/14 
 Pct Recovery = 94%  Analysis Date = 08/06/14 
 Pct Recovery = 94%  Analysis Date = 08/06/14 
 Pct Recovery = 94%  Analysis Date = 08/01/14 
 Pct Recovery = 94%  Analysis Date = 08/01/14 
 Pct Recovery = 94%  Analysis Date = 07/28/14 
 Pct Recovery = 94%  Analysis Date = 07/28/14 
 Pct Recovery = 94%  Analysis Date = 07/24/14 
 Pct Recovery = 94%  Analysis Date = 07/24/14 
 Pct Recovery = 94%  Analysis Date = 07/20/14 
 Pct Recovery = 93%  Analysis Date = 07/20/14 
 Pct Recovery = 93%  Analysis Date = 07/16/14 
 Pct Recovery = 93%  Analysis Date = 07/16/14 
 Pct Recovery = 93%  Analysis Date = 07/12/14 
 Pct Recovery = 93%  Analysis Date = 07/12/14 
 Pct Recovery = 93%  Analysis Date = 07/08/14 
 Pct Recovery = 93%  Analysis Date = 07/08/14 
 Pct Recovery = 93%  Analysis Date = 07/03/14 
 Pct Recovery = 93%  Analysis Date = 07/03/14 
 Pct Recovery = 93%  Analysis Date = 06/29/14 
 Pct Recovery = 93%  Analysis Date = 06/29/14 
 Pct Recovery = 93%  Analysis Date = 06/25/14 
 Pct Recovery = 93%  Analysis Date = 06/25/14 
 Pct Recovery = 93%  Analysis Date = 06/21/14 
 Pct Recovery = 93%  Analysis Date = 06/21/14 
 Pct Recovery = 93%  Analysis Date = 06/17/14 
 Pct Recovery = 93%  Analysis Date = 06/17/14 
 Pct Recovery = 93%  Analysis Date = 06/13/14 
 Pct Recovery = 93%  Analysis Date = 06/13/14 
 Pct Recovery = 93%  Analysis Date = 06/09/14 
 Pct Recovery = 93%  Analysis Date = 06/09/14 
 Pct Recovery = 93%  Analysis Date = 06/04/14 
 Pct Recovery = 92%  Analysis Date = 06/04/14 
 Pct Recovery = 92%  Analysis Date = 05/31/14 
 Pct Recovery = 92%  Analysis Date = 05/31/14 
 Pct Recovery = 92%  Analysis Date = 05/27/14 
 Pct Recovery = 92%  Analysis Date = 05/27/14 
 Pct Recovery = 92%  Analysis Date = 05/23/14 
 Pct Recovery = 92%  Analysis Date = 05/23/14 
 Pct Recovery = 92%  Analysis Date = 05/19/14 
 Pct Recovery = 92%  Analysis Date = 05/19/14 
 Pct Recovery = 92%  Analysis Date = 05/15/14 
 Pct Recovery = 92%  Analysis Date = 05/15/14 
 Pct Recovery = 92%  Analysis Date = 05/11/14 
 Pct Recovery = 92%  Analysis Date = 05/11/14 
 Pct Recovery = 92%  Analysis Date = 05/07/14 
 Pct Recovery = 92%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
BUTANAL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 30 90% 7% 87% 8%
Total 30 90% 7% 87% 8%

Sample Statistics
BUTANAL

Characteristic N % % Basis
Plotted 30 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 30 .  
False Negatives 0 0% 0 out of 30
Not Spiked 18 .  
False Positives 0 0% 0 out of 18

BQS OBSP Determination:
BUTANOL
METHOD: 4437 , TESTIDCODE: 77034GM016
Open Data Set

 Analysis Date = 07/06/16 
 SpikeMix = Accu 216041354: 40 µl & NSI 041516: 40 µl & NSI 041416HVOC: 40 µl 
 Pct Recovery = 97%  Analysis Date = 07/29/16 
 SpikeMix = Supelco LC20145V: 40 µl & NSI 041516: 40 µl & NSI 041416HVOC: 40 µl 
 Pct Recovery = 96%  Analysis Date = 08/11/16 
 SpikeMix = Phenova B20160303: 25 µl & Supelco LC20145V: 25 µl & NSI 041416HVOC: 25 µl 
 Pct Recovery = 87%  Analysis Date = 05/21/16 
 SpikeMix = Supelco LC20145V: 25 µl & NSI 041516: 25 µl & NSI 041416HVOC: 25 µl 
 Pct Recovery = 91%  Analysis Date = 01/10/15 
 SpikeMix = Abs 032014: 20 µl & ERA 0321-14-05A: 20 µl 
 Pct Recovery = 97%  Analysis Date = 08/13/14 
 SpikeMix = ERA 0321-14-05: 20 µl & Accu 214031128: 20 µl 
 Pct Recovery = 97%  Analysis Date = 07/11/14 
 SpikeMix = ChemService 2615700: 20 µl & Accu 214031128: 20 µl 
 Pct Recovery = 82%  Analysis Date = 07/03/14 
 SpikeMix = Abs 032014: 20 µl & ChemService 2615700: 20 µl 
 Pct Recovery = 95%  Analysis Date = 06/07/14 
 SpikeMix = ChemService 2615700: 20 µl & Supelco LC06437: 20 µl 
 Pct Recovery = 106%  Analysis Date = 06/06/14 
 SpikeMix = NSI 031814: 20 µl & ChemService 2615700: 20 µl 
 Pct Recovery = 103%  Analysis Date = 06/26/15 
 SpikeMix = ChemService 3818700: 25 µl & Accu 215041338: 25 µl 
 Pct Recovery = 104%  Analysis Date = 06/25/15 
 SpikeMix = ChemService 3818700: 25 µl & NSI 050515HVOC: 25 µl 
 Pct Recovery = 95%  Analysis Date = 01/22/16 
 SpikeMix = NSI 050515HVOC: 25 µl & ERA 0601-15-05: 25 µl 
 Pct Recovery = 98%  Analysis Date = 10/09/15 
 SpikeMix = ERA 0601-15-05: 25 µl & Accu 215041338: 25 µl 
 Pct Recovery = 79%  Analysis Date = 08/12/16 
 SpikeMix = Accu 216041354: 15 µl & Abs 060916HVOC: 15 µl 
 Pct Recovery = 84%  Analysis Date = 07/06/16 
 SpikeMix = Phenova B20160303: 15 µl & Accu 216041354: 15 µl & NSI 041416HVOC: 15 µl 
 Pct Recovery = 70%  Analysis Date = 06/23/16 
 SpikeMix = . 
 Pct Recovery = 47%  Analysis Date = 05/20/16 
 SpikeMix = Accu 216041354: 15 µl & NSI 041516: 15 µl & Accu 216041225: 15 µl 
 Pct Recovery = 91%  Analysis Date = 07/27/16 
 SpikeMix = ChemService 5082800: 15 µl & Supelco LC20145V: 15 µl & Accu 216041225: 15 µl 
 Pct Recovery = 71%  Analysis Date = 04/28/16 
 SpikeMix = ChemService 3818700: 15 µl & Supelco LC13544: 15 µl 
 Pct Recovery = 75%  Analysis Date = 06/16/15 
 SpikeMix = ChemService 3818700: 15 µl & NSI 050515HVOC: 15 µl 
 Pct Recovery = 76%  Analysis Date = 05/14/15 
 SpikeMix = ChemService 3818700: 15 µl & Supelco LC13544: 15 µl 
 Pct Recovery = 111%  Analysis Date = 09/24/15 
 SpikeMix = Abs 040315: 15 µl & ERA 0601-15-05: 15 µl 
 Pct Recovery = 95%  Analysis Date = 08/24/15 
 SpikeMix = ERA 0601-15-05: 15 µl & Supelco LC13544: 15 µl 
 Pct Recovery = 72%  Analysis Date = 04/25/15 
 SpikeMix = Abs 032014: 10 µl & ERA 0321-14-05A: 10 µl 
 Pct Recovery = 110%  Analysis Date = 10/21/14 
 SpikeMix = ERA 0321-14-05A: 10 µl & Accu 214031128: 10 µl 
 Pct Recovery = 83%  Analysis Date = 09/06/14 
 SpikeMix = ERA 0321-14-05: 10 µl & Supelco LC06437: 10 µl 
 Pct Recovery = 134%  Analysis Date = 11/22/14 
 SpikeMix = ChemService 2615700: 10 µl & Supelco LC06437: 10 µl 
 Pct Recovery = 85%  Analysis Date = 07/30/14 
 SpikeMix = NSI 031814: 10 µl & ChemService 2615700: 10 µl 
 Pct Recovery = 86%  Analysis Date = 05/20/14 
 SpikeMix = ChemService 2615700: 10 µl & Accu 214031128: 10 µl 
 Pct Recovery = 78%  Analysis Date = 04/09/16 
 SpikeMix = Abs 040315: 10 µl & ChemService 3818700: 10 µl 
 Pct Recovery = 101%  Analysis Date = 12/10/15 
 SpikeMix = ChemService 3818700: 10 µl & Supelco LC13544: 10 µl 
 Pct Recovery = 90%  Analysis Date = 10/23/15 
 SpikeMix = Abs 040315: 10 µl & ChemService 3818700: 10 µl 
 Pct Recovery = 78%  Analysis Date = 05/20/15 
 SpikeMix = ChemService 3818700: 10 µl & Accu 215041338: 10 µl 
 Pct Recovery = 138%  Analysis Date = 02/12/16 
 SpikeMix = ERA 0601-15-05: 10 µl & Accu 215041338: 10 µl 
 Pct Recovery = 93%  Analysis Date = 12/05/15 
 SpikeMix = NSI 050515HVOC: 10 µl & ERA 0601-15-05: 10 µl 
 Pct Recovery = 73%  Analysis Date = 11/14/15 
 SpikeMix = ERA 0601-15-05: 10 µl 
 Pct Recovery = 75%  Analysis Date = 08/12/16 
 Pct Recovery = 82%  Analysis Date = 08/07/16 
 Pct Recovery = 82%  Analysis Date = 08/07/16 
 Pct Recovery = 82%  Analysis Date = 08/03/16 
 Pct Recovery = 82%  Analysis Date = 08/03/16 
 Pct Recovery = 82%  Analysis Date = 07/30/16 
 Pct Recovery = 82%  Analysis Date = 07/30/16 
 Pct Recovery = 82%  Analysis Date = 07/26/16 
 Pct Recovery = 82%  Analysis Date = 07/26/16 
 Pct Recovery = 82%  Analysis Date = 07/22/16 
 Pct Recovery = 82%  Analysis Date = 07/22/16 
 Pct Recovery = 82%  Analysis Date = 07/18/16 
 Pct Recovery = 82%  Analysis Date = 07/18/16 
 Pct Recovery = 82%  Analysis Date = 07/14/16 
 Pct Recovery = 83%  Analysis Date = 07/14/16 
 Pct Recovery = 83%  Analysis Date = 07/10/16 
 Pct Recovery = 83%  Analysis Date = 07/10/16 
 Pct Recovery = 83%  Analysis Date = 07/06/16 
 Pct Recovery = 83%  Analysis Date = 07/06/16 
 Pct Recovery = 83%  Analysis Date = 07/02/16 
 Pct Recovery = 83%  Analysis Date = 07/02/16 
 Pct Recovery = 83%  Analysis Date = 06/28/16 
 Pct Recovery = 83%  Analysis Date = 06/28/16 
 Pct Recovery = 83%  Analysis Date = 06/24/16 
 Pct Recovery = 83%  Analysis Date = 06/24/16 
 Pct Recovery = 83%  Analysis Date = 06/20/16 
 Pct Recovery = 83%  Analysis Date = 06/20/16 
 Pct Recovery = 83%  Analysis Date = 06/15/16 
 Pct Recovery = 83%  Analysis Date = 06/15/16 
 Pct Recovery = 83%  Analysis Date = 06/11/16 
 Pct Recovery = 83%  Analysis Date = 06/11/16 
 Pct Recovery = 83%  Analysis Date = 06/07/16 
 Pct Recovery = 83%  Analysis Date = 06/07/16 
 Pct Recovery = 83%  Analysis Date = 06/03/16 
 Pct Recovery = 83%  Analysis Date = 06/03/16 
 Pct Recovery = 83%  Analysis Date = 05/30/16 
 Pct Recovery = 83%  Analysis Date = 05/30/16 
 Pct Recovery = 83%  Analysis Date = 05/26/16 
 Pct Recovery = 83%  Analysis Date = 05/26/16 
 Pct Recovery = 83%  Analysis Date = 05/22/16 
 Pct Recovery = 83%  Analysis Date = 05/22/16 
 Pct Recovery = 83%  Analysis Date = 05/18/16 
 Pct Recovery = 83%  Analysis Date = 05/18/16 
 Pct Recovery = 83%  Analysis Date = 05/14/16 
 Pct Recovery = 83%  Analysis Date = 05/14/16 
 Pct Recovery = 83%  Analysis Date = 05/10/16 
 Pct Recovery = 84%  Analysis Date = 05/10/16 
 Pct Recovery = 84%  Analysis Date = 05/06/16 
 Pct Recovery = 84%  Analysis Date = 05/06/16 
 Pct Recovery = 84%  Analysis Date = 05/02/16 
 Pct Recovery = 84%  Analysis Date = 05/02/16 
 Pct Recovery = 84%  Analysis Date = 04/28/16 
 Pct Recovery = 84%  Analysis Date = 04/28/16 
 Pct Recovery = 84%  Analysis Date = 04/23/16 
 Pct Recovery = 84%  Analysis Date = 04/23/16 
 Pct Recovery = 84%  Analysis Date = 04/19/16 
 Pct Recovery = 84%  Analysis Date = 04/19/16 
 Pct Recovery = 84%  Analysis Date = 04/15/16 
 Pct Recovery = 84%  Analysis Date = 04/15/16 
 Pct Recovery = 84%  Analysis Date = 04/11/16 
 Pct Recovery = 84%  Analysis Date = 04/11/16 
 Pct Recovery = 84%  Analysis Date = 04/07/16 
 Pct Recovery = 84%  Analysis Date = 04/07/16 
 Pct Recovery = 84%  Analysis Date = 04/03/16 
 Pct Recovery = 84%  Analysis Date = 04/03/16 
 Pct Recovery = 84%  Analysis Date = 03/30/16 
 Pct Recovery = 84%  Analysis Date = 03/30/16 
 Pct Recovery = 84%  Analysis Date = 03/26/16 
 Pct Recovery = 84%  Analysis Date = 03/26/16 
 Pct Recovery = 84%  Analysis Date = 03/22/16 
 Pct Recovery = 84%  Analysis Date = 03/22/16 
 Pct Recovery = 84%  Analysis Date = 03/18/16 
 Pct Recovery = 84%  Analysis Date = 03/18/16 
 Pct Recovery = 84%  Analysis Date = 03/14/16 
 Pct Recovery = 84%  Analysis Date = 03/14/16 
 Pct Recovery = 84%  Analysis Date = 03/10/16 
 Pct Recovery = 84%  Analysis Date = 03/10/16 
 Pct Recovery = 84%  Analysis Date = 03/06/16 
 Pct Recovery = 84%  Analysis Date = 03/06/16 
 Pct Recovery = 84%  Analysis Date = 03/02/16 
 Pct Recovery = 84%  Analysis Date = 03/02/16 
 Pct Recovery = 84%  Analysis Date = 02/26/16 
 Pct Recovery = 85%  Analysis Date = 02/26/16 
 Pct Recovery = 85%  Analysis Date = 02/22/16 
 Pct Recovery = 85%  Analysis Date = 02/22/16 
 Pct Recovery = 85%  Analysis Date = 02/18/16 
 Pct Recovery = 85%  Analysis Date = 02/18/16 
 Pct Recovery = 85%  Analysis Date = 02/14/16 
 Pct Recovery = 85%  Analysis Date = 02/14/16 
 Pct Recovery = 85%  Analysis Date = 02/10/16 
 Pct Recovery = 85%  Analysis Date = 02/10/16 
 Pct Recovery = 85%  Analysis Date = 02/06/16 
 Pct Recovery = 85%  Analysis Date = 02/06/16 
 Pct Recovery = 85%  Analysis Date = 02/02/16 
 Pct Recovery = 85%  Analysis Date = 02/02/16 
 Pct Recovery = 85%  Analysis Date = 01/29/16 
 Pct Recovery = 85%  Analysis Date = 01/29/16 
 Pct Recovery = 85%  Analysis Date = 01/25/16 
 Pct Recovery = 85%  Analysis Date = 01/25/16 
 Pct Recovery = 85%  Analysis Date = 01/21/16 
 Pct Recovery = 85%  Analysis Date = 01/21/16 
 Pct Recovery = 85%  Analysis Date = 01/17/16 
 Pct Recovery = 85%  Analysis Date = 01/17/16 
 Pct Recovery = 85%  Analysis Date = 01/13/16 
 Pct Recovery = 85%  Analysis Date = 01/13/16 
 Pct Recovery = 85%  Analysis Date = 01/09/16 
 Pct Recovery = 85%  Analysis Date = 01/09/16 
 Pct Recovery = 85%  Analysis Date = 01/04/16 
 Pct Recovery = 85%  Analysis Date = 01/04/16 
 Pct Recovery = 85%  Analysis Date = 12/31/15 
 Pct Recovery = 85%  Analysis Date = 12/31/15 
 Pct Recovery = 85%  Analysis Date = 12/27/15 
 Pct Recovery = 85%  Analysis Date = 12/27/15 
 Pct Recovery = 85%  Analysis Date = 12/23/15 
 Pct Recovery = 85%  Analysis Date = 12/23/15 
 Pct Recovery = 85%  Analysis Date = 12/19/15 
 Pct Recovery = 85%  Analysis Date = 12/19/15 
 Pct Recovery = 85%  Analysis Date = 12/15/15 
 Pct Recovery = 86%  Analysis Date = 12/15/15 
 Pct Recovery = 86%  Analysis Date = 12/11/15 
 Pct Recovery = 86%  Analysis Date = 12/11/15 
 Pct Recovery = 86%  Analysis Date = 12/07/15 
 Pct Recovery = 86%  Analysis Date = 12/07/15 
 Pct Recovery = 86%  Analysis Date = 12/03/15 
 Pct Recovery = 86%  Analysis Date = 12/03/15 
 Pct Recovery = 86%  Analysis Date = 11/29/15 
 Pct Recovery = 86%  Analysis Date = 11/29/15 
 Pct Recovery = 86%  Analysis Date = 11/25/15 
 Pct Recovery = 86%  Analysis Date = 11/25/15 
 Pct Recovery = 86%  Analysis Date = 11/21/15 
 Pct Recovery = 86%  Analysis Date = 11/21/15 
 Pct Recovery = 86%  Analysis Date = 11/17/15 
 Pct Recovery = 86%  Analysis Date = 11/17/15 
 Pct Recovery = 86%  Analysis Date = 11/12/15 
 Pct Recovery = 87%  Analysis Date = 11/12/15 
 Pct Recovery = 87%  Analysis Date = 11/08/15 
 Pct Recovery = 87%  Analysis Date = 11/08/15 
 Pct Recovery = 87%  Analysis Date = 11/04/15 
 Pct Recovery = 87%  Analysis Date = 11/04/15 
 Pct Recovery = 87%  Analysis Date = 10/31/15 
 Pct Recovery = 88%  Analysis Date = 10/31/15 
 Pct Recovery = 88%  Analysis Date = 10/27/15 
 Pct Recovery = 88%  Analysis Date = 10/27/15 
 Pct Recovery = 88%  Analysis Date = 10/23/15 
 Pct Recovery = 88%  Analysis Date = 10/23/15 
 Pct Recovery = 88%  Analysis Date = 10/19/15 
 Pct Recovery = 89%  Analysis Date = 10/19/15 
 Pct Recovery = 89%  Analysis Date = 10/15/15 
 Pct Recovery = 89%  Analysis Date = 10/15/15 
 Pct Recovery = 89%  Analysis Date = 10/11/15 
 Pct Recovery = 89%  Analysis Date = 10/11/15 
 Pct Recovery = 89%  Analysis Date = 10/07/15 
 Pct Recovery = 90%  Analysis Date = 10/07/15 
 Pct Recovery = 90%  Analysis Date = 10/03/15 
 Pct Recovery = 90%  Analysis Date = 10/03/15 
 Pct Recovery = 90%  Analysis Date = 09/29/15 
 Pct Recovery = 90%  Analysis Date = 09/29/15 
 Pct Recovery = 90%  Analysis Date = 09/25/15 
 Pct Recovery = 91%  Analysis Date = 09/25/15 
 Pct Recovery = 91%  Analysis Date = 09/21/15 
 Pct Recovery = 91%  Analysis Date = 09/21/15 
 Pct Recovery = 91%  Analysis Date = 09/16/15 
 Pct Recovery = 91%  Analysis Date = 09/16/15 
 Pct Recovery = 91%  Analysis Date = 09/12/15 
 Pct Recovery = 91%  Analysis Date = 09/12/15 
 Pct Recovery = 91%  Analysis Date = 09/08/15 
 Pct Recovery = 92%  Analysis Date = 09/08/15 
 Pct Recovery = 92%  Analysis Date = 09/04/15 
 Pct Recovery = 92%  Analysis Date = 09/04/15 
 Pct Recovery = 92%  Analysis Date = 08/31/15 
 Pct Recovery = 92%  Analysis Date = 08/31/15 
 Pct Recovery = 92%  Analysis Date = 08/27/15 
 Pct Recovery = 92%  Analysis Date = 08/27/15 
 Pct Recovery = 92%  Analysis Date = 08/23/15 
 Pct Recovery = 92%  Analysis Date = 08/23/15 
 Pct Recovery = 92%  Analysis Date = 08/19/15 
 Pct Recovery = 93%  Analysis Date = 08/19/15 
 Pct Recovery = 93%  Analysis Date = 08/15/15 
 Pct Recovery = 93%  Analysis Date = 08/15/15 
 Pct Recovery = 93%  Analysis Date = 08/11/15 
 Pct Recovery = 93%  Analysis Date = 08/11/15 
 Pct Recovery = 93%  Analysis Date = 08/07/15 
 Pct Recovery = 93%  Analysis Date = 08/07/15 
 Pct Recovery = 93%  Analysis Date = 08/03/15 
 Pct Recovery = 93%  Analysis Date = 08/03/15 
 Pct Recovery = 93%  Analysis Date = 07/30/15 
 Pct Recovery = 94%  Analysis Date = 07/30/15 
 Pct Recovery = 94%  Analysis Date = 07/25/15 
 Pct Recovery = 94%  Analysis Date = 07/25/15 
 Pct Recovery = 94%  Analysis Date = 07/21/15 
 Pct Recovery = 94%  Analysis Date = 07/21/15 
 Pct Recovery = 94%  Analysis Date = 07/17/15 
 Pct Recovery = 94%  Analysis Date = 07/17/15 
 Pct Recovery = 94%  Analysis Date = 07/13/15 
 Pct Recovery = 95%  Analysis Date = 07/13/15 
 Pct Recovery = 95%  Analysis Date = 07/09/15 
 Pct Recovery = 95%  Analysis Date = 07/09/15 
 Pct Recovery = 95%  Analysis Date = 07/05/15 
 Pct Recovery = 95%  Analysis Date = 07/05/15 
 Pct Recovery = 95%  Analysis Date = 07/01/15 
 Pct Recovery = 95%  Analysis Date = 07/01/15 
 Pct Recovery = 95%  Analysis Date = 06/27/15 
 Pct Recovery = 95%  Analysis Date = 06/27/15 
 Pct Recovery = 95%  Analysis Date = 06/23/15 
 Pct Recovery = 96%  Analysis Date = 06/23/15 
 Pct Recovery = 96%  Analysis Date = 06/19/15 
 Pct Recovery = 96%  Analysis Date = 06/19/15 
 Pct Recovery = 96%  Analysis Date = 06/15/15 
 Pct Recovery = 96%  Analysis Date = 06/15/15 
 Pct Recovery = 96%  Analysis Date = 06/11/15 
 Pct Recovery = 96%  Analysis Date = 06/11/15 
 Pct Recovery = 96%  Analysis Date = 06/07/15 
 Pct Recovery = 96%  Analysis Date = 06/07/15 
 Pct Recovery = 96%  Analysis Date = 06/02/15 
 Pct Recovery = 96%  Analysis Date = 06/02/15 
 Pct Recovery = 96%  Analysis Date = 05/29/15 
 Pct Recovery = 97%  Analysis Date = 05/29/15 
 Pct Recovery = 97%  Analysis Date = 05/25/15 
 Pct Recovery = 97%  Analysis Date = 05/25/15 
 Pct Recovery = 97%  Analysis Date = 05/21/15 
 Pct Recovery = 97%  Analysis Date = 05/21/15 
 Pct Recovery = 97%  Analysis Date = 05/17/15 
 Pct Recovery = 97%  Analysis Date = 05/17/15 
 Pct Recovery = 97%  Analysis Date = 05/13/15 
 Pct Recovery = 97%  Analysis Date = 05/13/15 
 Pct Recovery = 97%  Analysis Date = 05/09/15 
 Pct Recovery = 97%  Analysis Date = 05/09/15 
 Pct Recovery = 97%  Analysis Date = 05/05/15 
 Pct Recovery = 97%  Analysis Date = 05/05/15 
 Pct Recovery = 97%  Analysis Date = 05/01/15 
 Pct Recovery = 97%  Analysis Date = 05/01/15 
 Pct Recovery = 97%  Analysis Date = 04/27/15 
 Pct Recovery = 97%  Analysis Date = 04/27/15 
 Pct Recovery = 97%  Analysis Date = 04/23/15 
 Pct Recovery = 97%  Analysis Date = 04/23/15 
 Pct Recovery = 97%  Analysis Date = 04/19/15 
 Pct Recovery = 97%  Analysis Date = 04/19/15 
 Pct Recovery = 97%  Analysis Date = 04/15/15 
 Pct Recovery = 97%  Analysis Date = 04/15/15 
 Pct Recovery = 97%  Analysis Date = 04/11/15 
 Pct Recovery = 97%  Analysis Date = 04/11/15 
 Pct Recovery = 97%  Analysis Date = 04/06/15 
 Pct Recovery = 97%  Analysis Date = 04/06/15 
 Pct Recovery = 97%  Analysis Date = 04/02/15 
 Pct Recovery = 97%  Analysis Date = 04/02/15 
 Pct Recovery = 97%  Analysis Date = 03/29/15 
 Pct Recovery = 97%  Analysis Date = 03/29/15 
 Pct Recovery = 97%  Analysis Date = 03/25/15 
 Pct Recovery = 97%  Analysis Date = 03/25/15 
 Pct Recovery = 97%  Analysis Date = 03/21/15 
 Pct Recovery = 98%  Analysis Date = 03/21/15 
 Pct Recovery = 98%  Analysis Date = 03/17/15 
 Pct Recovery = 98%  Analysis Date = 03/17/15 
 Pct Recovery = 98%  Analysis Date = 03/13/15 
 Pct Recovery = 98%  Analysis Date = 03/13/15 
 Pct Recovery = 98%  Analysis Date = 03/09/15 
 Pct Recovery = 98%  Analysis Date = 03/09/15 
 Pct Recovery = 98%  Analysis Date = 03/05/15 
 Pct Recovery = 98%  Analysis Date = 03/05/15 
 Pct Recovery = 98%  Analysis Date = 03/01/15 
 Pct Recovery = 98%  Analysis Date = 03/01/15 
 Pct Recovery = 98%  Analysis Date = 02/25/15 
 Pct Recovery = 98%  Analysis Date = 02/25/15 
 Pct Recovery = 98%  Analysis Date = 02/21/15 
 Pct Recovery = 98%  Analysis Date = 02/21/15 
 Pct Recovery = 98%  Analysis Date = 02/17/15 
 Pct Recovery = 98%  Analysis Date = 02/17/15 
 Pct Recovery = 98%  Analysis Date = 02/12/15 
 Pct Recovery = 98%  Analysis Date = 02/12/15 
 Pct Recovery = 98%  Analysis Date = 02/08/15 
 Pct Recovery = 98%  Analysis Date = 02/08/15 
 Pct Recovery = 98%  Analysis Date = 02/04/15 
 Pct Recovery = 98%  Analysis Date = 02/04/15 
 Pct Recovery = 98%  Analysis Date = 01/31/15 
 Pct Recovery = 98%  Analysis Date = 01/31/15 
 Pct Recovery = 98%  Analysis Date = 01/27/15 
 Pct Recovery = 98%  Analysis Date = 01/27/15 
 Pct Recovery = 98%  Analysis Date = 01/23/15 
 Pct Recovery = 98%  Analysis Date = 01/23/15 
 Pct Recovery = 98%  Analysis Date = 01/19/15 
 Pct Recovery = 98%  Analysis Date = 01/19/15 
 Pct Recovery = 98%  Analysis Date = 01/15/15 
 Pct Recovery = 98%  Analysis Date = 01/15/15 
 Pct Recovery = 98%  Analysis Date = 01/11/15 
 Pct Recovery = 98%  Analysis Date = 01/11/15 
 Pct Recovery = 98%  Analysis Date = 01/07/15 
 Pct Recovery = 98%  Analysis Date = 01/07/15 
 Pct Recovery = 98%  Analysis Date = 01/03/15 
 Pct Recovery = 98%  Analysis Date = 01/03/15 
 Pct Recovery = 98%  Analysis Date = 12/30/14 
 Pct Recovery = 98%  Analysis Date = 12/30/14 
 Pct Recovery = 98%  Analysis Date = 12/26/14 
 Pct Recovery = 98%  Analysis Date = 12/26/14 
 Pct Recovery = 98%  Analysis Date = 12/21/14 
 Pct Recovery = 98%  Analysis Date = 12/21/14 
 Pct Recovery = 98%  Analysis Date = 12/17/14 
 Pct Recovery = 98%  Analysis Date = 12/17/14 
 Pct Recovery = 98%  Analysis Date = 12/13/14 
 Pct Recovery = 98%  Analysis Date = 12/13/14 
 Pct Recovery = 98%  Analysis Date = 12/09/14 
 Pct Recovery = 98%  Analysis Date = 12/09/14 
 Pct Recovery = 98%  Analysis Date = 12/05/14 
 Pct Recovery = 98%  Analysis Date = 12/05/14 
 Pct Recovery = 98%  Analysis Date = 12/01/14 
 Pct Recovery = 98%  Analysis Date = 12/01/14 
 Pct Recovery = 98%  Analysis Date = 11/27/14 
 Pct Recovery = 98%  Analysis Date = 11/27/14 
 Pct Recovery = 98%  Analysis Date = 11/23/14 
 Pct Recovery = 99%  Analysis Date = 11/23/14 
 Pct Recovery = 99%  Analysis Date = 11/19/14 
 Pct Recovery = 98%  Analysis Date = 11/19/14 
 Pct Recovery = 98%  Analysis Date = 11/15/14 
 Pct Recovery = 98%  Analysis Date = 11/15/14 
 Pct Recovery = 98%  Analysis Date = 11/11/14 
 Pct Recovery = 98%  Analysis Date = 11/11/14 
 Pct Recovery = 98%  Analysis Date = 11/07/14 
 Pct Recovery = 98%  Analysis Date = 11/07/14 
 Pct Recovery = 98%  Analysis Date = 11/03/14 
 Pct Recovery = 98%  Analysis Date = 11/03/14 
 Pct Recovery = 98%  Analysis Date = 10/30/14 
 Pct Recovery = 98%  Analysis Date = 10/30/14 
 Pct Recovery = 98%  Analysis Date = 10/25/14 
 Pct Recovery = 98%  Analysis Date = 10/25/14 
 Pct Recovery = 98%  Analysis Date = 10/21/14 
 Pct Recovery = 98%  Analysis Date = 10/21/14 
 Pct Recovery = 98%  Analysis Date = 10/17/14 
 Pct Recovery = 98%  Analysis Date = 10/17/14 
 Pct Recovery = 98%  Analysis Date = 10/13/14 
 Pct Recovery = 97%  Analysis Date = 10/13/14 
 Pct Recovery = 97%  Analysis Date = 10/09/14 
 Pct Recovery = 97%  Analysis Date = 10/09/14 
 Pct Recovery = 97%  Analysis Date = 10/05/14 
 Pct Recovery = 97%  Analysis Date = 10/05/14 
 Pct Recovery = 97%  Analysis Date = 10/01/14 
 Pct Recovery = 97%  Analysis Date = 10/01/14 
 Pct Recovery = 97%  Analysis Date = 09/27/14 
 Pct Recovery = 97%  Analysis Date = 09/27/14 
 Pct Recovery = 97%  Analysis Date = 09/23/14 
 Pct Recovery = 97%  Analysis Date = 09/23/14 
 Pct Recovery = 97%  Analysis Date = 09/19/14 
 Pct Recovery = 97%  Analysis Date = 09/19/14 
 Pct Recovery = 97%  Analysis Date = 09/15/14 
 Pct Recovery = 97%  Analysis Date = 09/15/14 
 Pct Recovery = 97%  Analysis Date = 09/11/14 
 Pct Recovery = 97%  Analysis Date = 09/11/14 
 Pct Recovery = 97%  Analysis Date = 09/07/14 
 Pct Recovery = 96%  Analysis Date = 09/07/14 
 Pct Recovery = 96%  Analysis Date = 09/02/14 
 Pct Recovery = 96%  Analysis Date = 09/02/14 
 Pct Recovery = 96%  Analysis Date = 08/29/14 
 Pct Recovery = 96%  Analysis Date = 08/29/14 
 Pct Recovery = 96%  Analysis Date = 08/25/14 
 Pct Recovery = 96%  Analysis Date = 08/25/14 
 Pct Recovery = 96%  Analysis Date = 08/21/14 
 Pct Recovery = 96%  Analysis Date = 08/21/14 
 Pct Recovery = 96%  Analysis Date = 08/17/14 
 Pct Recovery = 96%  Analysis Date = 08/17/14 
 Pct Recovery = 96%  Analysis Date = 08/13/14 
 Pct Recovery = 96%  Analysis Date = 08/13/14 
 Pct Recovery = 96%  Analysis Date = 08/09/14 
 Pct Recovery = 96%  Analysis Date = 08/09/14 
 Pct Recovery = 96%  Analysis Date = 08/05/14 
 Pct Recovery = 96%  Analysis Date = 08/05/14 
 Pct Recovery = 96%  Analysis Date = 08/01/14 
 Pct Recovery = 96%  Analysis Date = 08/01/14 
 Pct Recovery = 96%  Analysis Date = 07/28/14 
 Pct Recovery = 95%  Analysis Date = 07/28/14 
 Pct Recovery = 95%  Analysis Date = 07/24/14 
 Pct Recovery = 95%  Analysis Date = 07/24/14 
 Pct Recovery = 95%  Analysis Date = 07/20/14 
 Pct Recovery = 95%  Analysis Date = 07/20/14 
 Pct Recovery = 95%  Analysis Date = 07/16/14 
 Pct Recovery = 95%  Analysis Date = 07/16/14 
 Pct Recovery = 95%  Analysis Date = 07/11/14 
 Pct Recovery = 95%  Analysis Date = 07/11/14 
 Pct Recovery = 95%  Analysis Date = 07/07/14 
 Pct Recovery = 95%  Analysis Date = 07/07/14 
 Pct Recovery = 95%  Analysis Date = 07/03/14 
 Pct Recovery = 95%  Analysis Date = 07/03/14 
 Pct Recovery = 95%  Analysis Date = 06/29/14 
 Pct Recovery = 95%  Analysis Date = 06/29/14 
 Pct Recovery = 95%  Analysis Date = 06/25/14 
 Pct Recovery = 95%  Analysis Date = 06/25/14 
 Pct Recovery = 95%  Analysis Date = 06/21/14 
 Pct Recovery = 94%  Analysis Date = 06/21/14 
 Pct Recovery = 94%  Analysis Date = 06/17/14 
 Pct Recovery = 94%  Analysis Date = 06/17/14 
 Pct Recovery = 94%  Analysis Date = 06/13/14 
 Pct Recovery = 94%  Analysis Date = 06/13/14 
 Pct Recovery = 94%  Analysis Date = 06/09/14 
 Pct Recovery = 94%  Analysis Date = 06/09/14 
 Pct Recovery = 94%  Analysis Date = 06/05/14 
 Pct Recovery = 94%  Analysis Date = 06/05/14 
 Pct Recovery = 94%  Analysis Date = 06/01/14 
 Pct Recovery = 94%  Analysis Date = 06/01/14 
 Pct Recovery = 94%  Analysis Date = 05/28/14 
 Pct Recovery = 94%  Analysis Date = 05/28/14 
 Pct Recovery = 94%  Analysis Date = 05/24/14 
 Pct Recovery = 94%  Analysis Date = 05/24/14 
 Pct Recovery = 94%  Analysis Date = 05/20/14 
 Pct Recovery = 94%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
BUTANOL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 37 90% 17% 91% 14%
Total 37 90% 17% 91% 14%

Sample Statistics
BUTANOL

Characteristic N % % Basis
Plotted 37 97% Spiked
Estimated Values 11 29% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 38 .  
False Negatives 1 3% 1 out of 38
Not Spiked 17 .  
False Positives 1 6% 1 out of 17

BQS OBSP Determination:
CHLOROPICRIN
METHOD: 4437 , TESTIDCODE: 77548GM016
Open Data Set

 Analysis Date = 07/29/16 
 SpikeMix = Supelco LC20145V: 40 µl & NSI 041516: 40 µl & NSI 041416HVOC: 40 µl 
 Pct Recovery = 98%  Analysis Date = 07/06/16 
 SpikeMix = Accu 216041354: 40 µl & NSI 041516: 40 µl & NSI 041416HVOC: 40 µl 
 Pct Recovery = 93%  Analysis Date = 06/29/16 
 SpikeMix = NSI 041516: 40 µl & ChemService 5082800: 40 µl 
 Pct Recovery = 81%  Analysis Date = 08/13/14 
 SpikeMix = ERA 0321-14-05: 20 µl & Accu 214031128: 20 µl 
 Pct Recovery = 88%  Analysis Date = 07/23/14 
 SpikeMix = Accu 214031128: 20 µl & Abs 032014: 20 µl 
 Pct Recovery = 97%  Analysis Date = 07/11/14 
 SpikeMix = ChemService 2615700: 20 µl & Accu 214031128: 20 µl 
 Pct Recovery = 100%  Analysis Date = 05/07/14 
 SpikeMix = NSI 031814: 20 µl & Accu 214031128: 20 µl 
 Pct Recovery = 93%  Analysis Date = 07/14/16 
 SpikeMix = NSI 041516: 25 µl & ChemService 5082800: 25 µl & NSI 041416HVOC: 25 µl 
 Pct Recovery = 76%  Analysis Date = 05/21/16 
 SpikeMix = Supelco LC20145V: 25 µl & NSI 041516: 25 µl & NSI 041416HVOC: 25 µl 
 Pct Recovery = 97%  Analysis Date = 03/19/15 
 SpikeMix = Supelco LC06437: 20 µl & NSI 031814: 20 µl 
 Pct Recovery = 82%  Analysis Date = 08/20/14 
 SpikeMix = Supelco LC06437: 20 µl & Abs 032014: 20 µl 
 Pct Recovery = 109%  Analysis Date = 06/07/14 
 SpikeMix = ChemService 2615700: 20 µl & Supelco LC06437: 20 µl 
 Pct Recovery = 88%  Analysis Date = 01/22/16 
 SpikeMix = NSI 050515HVOC: 25 µl & ERA 0601-15-05: 25 µl 
 Pct Recovery = 126%  Analysis Date = 10/09/15 
 SpikeMix = Supelco LC13544: 25 µl & NSI 050515HVOC: 25 µl 
 Pct Recovery = 100%  Analysis Date = 06/25/15 
 SpikeMix = ChemService 3818700: 25 µl & NSI 050515HVOC: 25 µl 
 Pct Recovery = 111%  Analysis Date = 08/12/16 
 SpikeMix = Accu 216041354: 15 µl & Abs 060916HVOC: 15 µl 
 Pct Recovery = 93%  Analysis Date = 06/03/16 
 SpikeMix = NSI 041516: 15 µl & Phenova B20160303: 15 µl & NSI 041416HVOC: 15 µl 
 Pct Recovery = 86%  Analysis Date = 05/20/16 
 SpikeMix = Accu 216041354: 15 µl & NSI 041516: 15 µl & Accu 216041225: 15 µl 
 Pct Recovery = 97%  Analysis Date = 11/25/15 
 SpikeMix = Accu 215041338: 15 µl & Abs 040315: 15 µl 
 Pct Recovery = 144%  Analysis Date = 09/24/15 
 SpikeMix = Abs 040315: 15 µl & ERA 0601-15-05: 15 µl 
 Pct Recovery = 141%  Analysis Date = 09/05/15 
 SpikeMix = Accu 215041338: 15 µl & NSI 050515HVOC: 15 µl 
 Pct Recovery = 128%  Analysis Date = 07/30/15 
 SpikeMix = Supelco LC13544: 15 µl & NSI 050515HVOC: 15 µl 
 Pct Recovery = 124%  Analysis Date = 06/16/15 
 SpikeMix = ChemService 3818700: 15 µl & NSI 050515HVOC: 15 µl 
 Pct Recovery = 117%  Analysis Date = 12/13/14 
 SpikeMix = Accu 214031128: 10 µl & NSI 031814: 10 µl 
 Pct Recovery = 84%  Analysis Date = 10/21/14 
 SpikeMix = ERA 0321-14-05A: 10 µl & Accu 214031128: 10 µl 
 Pct Recovery = 127%  Analysis Date = 09/11/14 
 SpikeMix = Accu 214031128: 10 µl & Abs 032014: 10 µl 
 Pct Recovery = 96%  Analysis Date = 05/20/14 
 SpikeMix = ChemService 2615700: 10 µl & Accu 214031128: 10 µl 
 Pct Recovery = 95%  Analysis Date = 11/22/14 
 SpikeMix = ChemService 2615700: 10 µl & Supelco LC06437: 10 µl 
 Pct Recovery = 99%  Analysis Date = 09/06/14 
 SpikeMix = ERA 0321-14-05: 10 µl & Supelco LC06437: 10 µl 
 Pct Recovery = 94%  Analysis Date = 06/17/14 
 SpikeMix = Supelco LC06437: 10 µl & Abs 032014: 10 µl 
 Pct Recovery = 81%  Analysis Date = 04/09/16 
 SpikeMix = Abs 040315: 10 µl & ChemService 3818700: 10 µl 
 Pct Recovery = 110%  Analysis Date = 03/22/16 
 SpikeMix = Supelco LC13544: 10 µl & NSI 050515HVOC: 10 µl 
 Pct Recovery = 126%  Analysis Date = 01/05/16 
 SpikeMix = Accu 215041338: 10 µl & Abs 040315: 10 µl 
 Pct Recovery = 122%  Analysis Date = 12/05/15 
 SpikeMix = NSI 050515HVOC: 10 µl & ERA 0601-15-05: 10 µl 
 Pct Recovery = 131%  Analysis Date = 10/23/15 
 SpikeMix = Abs 040315: 10 µl & ChemService 3818700: 10 µl 
 Pct Recovery = 144%  Analysis Date = 08/14/15 
 SpikeMix = Abs 040315: 10 µl & ERA 0601-15-05: 10 µl 
 Pct Recovery = 131%  Analysis Date = 05/05/15 
 SpikeMix = Supelco LC13544: 10 µl & Abs 040315: 10 µl 
 Pct Recovery = 149%  Analysis Date = 08/11/16 
 Pct Recovery = 84%  Analysis Date = 08/07/16 
 Pct Recovery = 85%  Analysis Date = 08/07/16 
 Pct Recovery = 85%  Analysis Date = 08/03/16 
 Pct Recovery = 86%  Analysis Date = 08/03/16 
 Pct Recovery = 86%  Analysis Date = 07/30/16 
 Pct Recovery = 87%  Analysis Date = 07/30/16 
 Pct Recovery = 87%  Analysis Date = 07/26/16 
 Pct Recovery = 87%  Analysis Date = 07/26/16 
 Pct Recovery = 87%  Analysis Date = 07/22/16 
 Pct Recovery = 88%  Analysis Date = 07/22/16 
 Pct Recovery = 88%  Analysis Date = 07/18/16 
 Pct Recovery = 89%  Analysis Date = 07/18/16 
 Pct Recovery = 89%  Analysis Date = 07/14/16 
 Pct Recovery = 90%  Analysis Date = 07/14/16 
 Pct Recovery = 90%  Analysis Date = 07/09/16 
 Pct Recovery = 90%  Analysis Date = 07/09/16 
 Pct Recovery = 90%  Analysis Date = 07/05/16 
 Pct Recovery = 91%  Analysis Date = 07/05/16 
 Pct Recovery = 91%  Analysis Date = 07/01/16 
 Pct Recovery = 92%  Analysis Date = 07/01/16 
 Pct Recovery = 92%  Analysis Date = 06/27/16 
 Pct Recovery = 93%  Analysis Date = 06/27/16 
 Pct Recovery = 93%  Analysis Date = 06/23/16 
 Pct Recovery = 93%  Analysis Date = 06/23/16 
 Pct Recovery = 93%  Analysis Date = 06/19/16 
 Pct Recovery = 94%  Analysis Date = 06/19/16 
 Pct Recovery = 94%  Analysis Date = 06/15/16 
 Pct Recovery = 95%  Analysis Date = 06/15/16 
 Pct Recovery = 95%  Analysis Date = 06/10/16 
 Pct Recovery = 96%  Analysis Date = 06/10/16 
 Pct Recovery = 96%  Analysis Date = 06/06/16 
 Pct Recovery = 96%  Analysis Date = 06/06/16 
 Pct Recovery = 96%  Analysis Date = 06/02/16 
 Pct Recovery = 97%  Analysis Date = 06/02/16 
 Pct Recovery = 97%  Analysis Date = 05/29/16 
 Pct Recovery = 98%  Analysis Date = 05/29/16 
 Pct Recovery = 98%  Analysis Date = 05/25/16 
 Pct Recovery = 98%  Analysis Date = 05/25/16 
 Pct Recovery = 98%  Analysis Date = 05/21/16 
 Pct Recovery = 99%  Analysis Date = 05/21/16 
 Pct Recovery = 99%  Analysis Date = 05/17/16 
 Pct Recovery = 100%  Analysis Date = 05/17/16 
 Pct Recovery = 100%  Analysis Date = 05/12/16 
 Pct Recovery = 101%  Analysis Date = 05/12/16 
 Pct Recovery = 101%  Analysis Date = 05/08/16 
 Pct Recovery = 101%  Analysis Date = 05/08/16 
 Pct Recovery = 101%  Analysis Date = 05/04/16 
 Pct Recovery = 102%  Analysis Date = 05/04/16 
 Pct Recovery = 102%  Analysis Date = 04/30/16 
 Pct Recovery = 103%  Analysis Date = 04/30/16 
 Pct Recovery = 103%  Analysis Date = 04/26/16 
 Pct Recovery = 103%  Analysis Date = 04/26/16 
 Pct Recovery = 103%  Analysis Date = 04/22/16 
 Pct Recovery = 104%  Analysis Date = 04/22/16 
 Pct Recovery = 104%  Analysis Date = 04/18/16 
 Pct Recovery = 105%  Analysis Date = 04/18/16 
 Pct Recovery = 105%  Analysis Date = 04/13/16 
 Pct Recovery = 105%  Analysis Date = 04/13/16 
 Pct Recovery = 105%  Analysis Date = 04/09/16 
 Pct Recovery = 106%  Analysis Date = 04/09/16 
 Pct Recovery = 106%  Analysis Date = 04/05/16 
 Pct Recovery = 107%  Analysis Date = 04/05/16 
 Pct Recovery = 107%  Analysis Date = 04/01/16 
 Pct Recovery = 108%  Analysis Date = 04/01/16 
 Pct Recovery = 108%  Analysis Date = 03/28/16 
 Pct Recovery = 108%  Analysis Date = 03/28/16 
 Pct Recovery = 108%  Analysis Date = 03/24/16 
 Pct Recovery = 109%  Analysis Date = 03/24/16 
 Pct Recovery = 109%  Analysis Date = 03/20/16 
 Pct Recovery = 110%  Analysis Date = 03/20/16 
 Pct Recovery = 110%  Analysis Date = 03/15/16 
 Pct Recovery = 110%  Analysis Date = 03/15/16 
 Pct Recovery = 110%  Analysis Date = 03/11/16 
 Pct Recovery = 111%  Analysis Date = 03/11/16 
 Pct Recovery = 111%  Analysis Date = 03/07/16 
 Pct Recovery = 111%  Analysis Date = 03/07/16 
 Pct Recovery = 111%  Analysis Date = 03/03/16 
 Pct Recovery = 112%  Analysis Date = 03/03/16 
 Pct Recovery = 112%  Analysis Date = 02/28/16 
 Pct Recovery = 112%  Analysis Date = 02/28/16 
 Pct Recovery = 112%  Analysis Date = 02/24/16 
 Pct Recovery = 113%  Analysis Date = 02/24/16 
 Pct Recovery = 113%  Analysis Date = 02/20/16 
 Pct Recovery = 113%  Analysis Date = 02/20/16 
 Pct Recovery = 113%  Analysis Date = 02/15/16 
 Pct Recovery = 114%  Analysis Date = 02/15/16 
 Pct Recovery = 114%  Analysis Date = 02/11/16 
 Pct Recovery = 114%  Analysis Date = 02/11/16 
 Pct Recovery = 114%  Analysis Date = 02/07/16 
 Pct Recovery = 115%  Analysis Date = 02/07/16 
 Pct Recovery = 115%  Analysis Date = 02/03/16 
 Pct Recovery = 116%  Analysis Date = 02/03/16 
 Pct Recovery = 116%  Analysis Date = 01/30/16 
 Pct Recovery = 116%  Analysis Date = 01/30/16 
 Pct Recovery = 116%  Analysis Date = 01/26/16 
 Pct Recovery = 117%  Analysis Date = 01/26/16 
 Pct Recovery = 117%  Analysis Date = 01/22/16 
 Pct Recovery = 117%  Analysis Date = 01/22/16 
 Pct Recovery = 117%  Analysis Date = 01/17/16 
 Pct Recovery = 118%  Analysis Date = 01/17/16 
 Pct Recovery = 118%  Analysis Date = 01/13/16 
 Pct Recovery = 118%  Analysis Date = 01/13/16 
 Pct Recovery = 118%  Analysis Date = 01/09/16 
 Pct Recovery = 119%  Analysis Date = 01/09/16 
 Pct Recovery = 119%  Analysis Date = 01/05/16 
 Pct Recovery = 119%  Analysis Date = 01/05/16 
 Pct Recovery = 119%  Analysis Date = 01/01/16 
 Pct Recovery = 120%  Analysis Date = 01/01/16 
 Pct Recovery = 120%  Analysis Date = 12/28/15 
 Pct Recovery = 120%  Analysis Date = 12/28/15 
 Pct Recovery = 120%  Analysis Date = 12/24/15 
 Pct Recovery = 121%  Analysis Date = 12/24/15 
 Pct Recovery = 121%  Analysis Date = 12/20/15 
 Pct Recovery = 121%  Analysis Date = 12/20/15 
 Pct Recovery = 121%  Analysis Date = 12/15/15 
 Pct Recovery = 122%  Analysis Date = 12/15/15 
 Pct Recovery = 122%  Analysis Date = 12/11/15 
 Pct Recovery = 123%  Analysis Date = 12/11/15 
 Pct Recovery = 123%  Analysis Date = 12/07/15 
 Pct Recovery = 123%  Analysis Date = 12/07/15 
 Pct Recovery = 123%  Analysis Date = 12/03/15 
 Pct Recovery = 124%  Analysis Date = 12/03/15 
 Pct Recovery = 124%  Analysis Date = 11/29/15 
 Pct Recovery = 124%  Analysis Date = 11/29/15 
 Pct Recovery = 124%  Analysis Date = 11/25/15 
 Pct Recovery = 125%  Analysis Date = 11/25/15 
 Pct Recovery = 125%  Analysis Date = 11/21/15 
 Pct Recovery = 125%  Analysis Date = 11/21/15 
 Pct Recovery = 125%  Analysis Date = 11/16/15 
 Pct Recovery = 125%  Analysis Date = 11/16/15 
 Pct Recovery = 125%  Analysis Date = 11/12/15 
 Pct Recovery = 125%  Analysis Date = 11/12/15 
 Pct Recovery = 125%  Analysis Date = 11/08/15 
 Pct Recovery = 125%  Analysis Date = 11/08/15 
 Pct Recovery = 125%  Analysis Date = 11/04/15 
 Pct Recovery = 125%  Analysis Date = 11/04/15 
 Pct Recovery = 125%  Analysis Date = 10/31/15 
 Pct Recovery = 125%  Analysis Date = 10/31/15 
 Pct Recovery = 125%  Analysis Date = 10/27/15 
 Pct Recovery = 126%  Analysis Date = 10/27/15 
 Pct Recovery = 126%  Analysis Date = 10/23/15 
 Pct Recovery = 126%  Analysis Date = 10/23/15 
 Pct Recovery = 126%  Analysis Date = 10/18/15 
 Pct Recovery = 126%  Analysis Date = 10/18/15 
 Pct Recovery = 126%  Analysis Date = 10/14/15 
 Pct Recovery = 126%  Analysis Date = 10/14/15 
 Pct Recovery = 126%  Analysis Date = 10/10/15 
 Pct Recovery = 126%  Analysis Date = 10/10/15 
 Pct Recovery = 126%  Analysis Date = 10/06/15 
 Pct Recovery = 126%  Analysis Date = 10/06/15 
 Pct Recovery = 126%  Analysis Date = 10/02/15 
 Pct Recovery = 126%  Analysis Date = 10/02/15 
 Pct Recovery = 126%  Analysis Date = 09/28/15 
 Pct Recovery = 126%  Analysis Date = 09/28/15 
 Pct Recovery = 126%  Analysis Date = 09/24/15 
 Pct Recovery = 125%  Analysis Date = 09/24/15 
 Pct Recovery = 125%  Analysis Date = 09/19/15 
 Pct Recovery = 125%  Analysis Date = 09/19/15 
 Pct Recovery = 125%  Analysis Date = 09/15/15 
 Pct Recovery = 125%  Analysis Date = 09/15/15 
 Pct Recovery = 125%  Analysis Date = 09/11/15 
 Pct Recovery = 125%  Analysis Date = 09/11/15 
 Pct Recovery = 125%  Analysis Date = 09/07/15 
 Pct Recovery = 125%  Analysis Date = 09/07/15 
 Pct Recovery = 125%  Analysis Date = 09/03/15 
 Pct Recovery = 125%  Analysis Date = 09/03/15 
 Pct Recovery = 125%  Analysis Date = 08/30/15 
 Pct Recovery = 124%  Analysis Date = 08/30/15 
 Pct Recovery = 124%  Analysis Date = 08/26/15 
 Pct Recovery = 124%  Analysis Date = 08/26/15 
 Pct Recovery = 124%  Analysis Date = 08/21/15 
 Pct Recovery = 124%  Analysis Date = 08/21/15 
 Pct Recovery = 124%  Analysis Date = 08/17/15 
 Pct Recovery = 124%  Analysis Date = 08/17/15 
 Pct Recovery = 124%  Analysis Date = 08/13/15 
 Pct Recovery = 124%  Analysis Date = 08/13/15 
 Pct Recovery = 124%  Analysis Date = 08/09/15 
 Pct Recovery = 123%  Analysis Date = 08/09/15 
 Pct Recovery = 123%  Analysis Date = 08/05/15 
 Pct Recovery = 123%  Analysis Date = 08/05/15 
 Pct Recovery = 123%  Analysis Date = 08/01/15 
 Pct Recovery = 123%  Analysis Date = 08/01/15 
 Pct Recovery = 123%  Analysis Date = 07/28/15 
 Pct Recovery = 122%  Analysis Date = 07/28/15 
 Pct Recovery = 122%  Analysis Date = 07/23/15 
 Pct Recovery = 122%  Analysis Date = 07/23/15 
 Pct Recovery = 122%  Analysis Date = 07/19/15 
 Pct Recovery = 122%  Analysis Date = 07/19/15 
 Pct Recovery = 122%  Analysis Date = 07/15/15 
 Pct Recovery = 121%  Analysis Date = 07/15/15 
 Pct Recovery = 121%  Analysis Date = 07/11/15 
 Pct Recovery = 121%  Analysis Date = 07/11/15 
 Pct Recovery = 121%  Analysis Date = 07/07/15 
 Pct Recovery = 120%  Analysis Date = 07/07/15 
 Pct Recovery = 120%  Analysis Date = 07/03/15 
 Pct Recovery = 120%  Analysis Date = 07/03/15 
 Pct Recovery = 120%  Analysis Date = 06/29/15 
 Pct Recovery = 120%  Analysis Date = 06/29/15 
 Pct Recovery = 120%  Analysis Date = 06/24/15 
 Pct Recovery = 119%  Analysis Date = 06/24/15 
 Pct Recovery = 119%  Analysis Date = 06/20/15 
 Pct Recovery = 119%  Analysis Date = 06/20/15 
 Pct Recovery = 119%  Analysis Date = 06/16/15 
 Pct Recovery = 118%  Analysis Date = 06/16/15 
 Pct Recovery = 118%  Analysis Date = 06/12/15 
 Pct Recovery = 118%  Analysis Date = 06/12/15 
 Pct Recovery = 118%  Analysis Date = 06/08/15 
 Pct Recovery = 118%  Analysis Date = 06/08/15 
 Pct Recovery = 118%  Analysis Date = 06/04/15 
 Pct Recovery = 117%  Analysis Date = 06/04/15 
 Pct Recovery = 117%  Analysis Date = 05/31/15 
 Pct Recovery = 117%  Analysis Date = 05/31/15 
 Pct Recovery = 117%  Analysis Date = 05/27/15 
 Pct Recovery = 117%  Analysis Date = 05/27/15 
 Pct Recovery = 117%  Analysis Date = 05/22/15 
 Pct Recovery = 116%  Analysis Date = 05/22/15 
 Pct Recovery = 116%  Analysis Date = 05/18/15 
 Pct Recovery = 116%  Analysis Date = 05/18/15 
 Pct Recovery = 116%  Analysis Date = 05/14/15 
 Pct Recovery = 115%  Analysis Date = 05/14/15 
 Pct Recovery = 115%  Analysis Date = 05/10/15 
 Pct Recovery = 115%  Analysis Date = 05/10/15 
 Pct Recovery = 115%  Analysis Date = 05/06/15 
 Pct Recovery = 115%  Analysis Date = 05/06/15 
 Pct Recovery = 115%  Analysis Date = 05/02/15 
 Pct Recovery = 114%  Analysis Date = 05/02/15 
 Pct Recovery = 114%  Analysis Date = 04/28/15 
 Pct Recovery = 114%  Analysis Date = 04/28/15 
 Pct Recovery = 114%  Analysis Date = 04/23/15 
 Pct Recovery = 114%  Analysis Date = 04/23/15 
 Pct Recovery = 114%  Analysis Date = 04/19/15 
 Pct Recovery = 113%  Analysis Date = 04/19/15 
 Pct Recovery = 113%  Analysis Date = 04/15/15 
 Pct Recovery = 113%  Analysis Date = 04/15/15 
 Pct Recovery = 113%  Analysis Date = 04/11/15 
 Pct Recovery = 113%  Analysis Date = 04/11/15 
 Pct Recovery = 113%  Analysis Date = 04/07/15 
 Pct Recovery = 113%  Analysis Date = 04/07/15 
 Pct Recovery = 113%  Analysis Date = 04/03/15 
 Pct Recovery = 112%  Analysis Date = 04/03/15 
 Pct Recovery = 112%  Analysis Date = 03/30/15 
 Pct Recovery = 112%  Analysis Date = 03/30/15 
 Pct Recovery = 112%  Analysis Date = 03/25/15 
 Pct Recovery = 112%  Analysis Date = 03/25/15 
 Pct Recovery = 112%  Analysis Date = 03/21/15 
 Pct Recovery = 111%  Analysis Date = 03/21/15 
 Pct Recovery = 111%  Analysis Date = 03/17/15 
 Pct Recovery = 111%  Analysis Date = 03/17/15 
 Pct Recovery = 111%  Analysis Date = 03/13/15 
 Pct Recovery = 111%  Analysis Date = 03/13/15 
 Pct Recovery = 111%  Analysis Date = 03/09/15 
 Pct Recovery = 110%  Analysis Date = 03/09/15 
 Pct Recovery = 110%  Analysis Date = 03/05/15 
 Pct Recovery = 110%  Analysis Date = 03/05/15 
 Pct Recovery = 110%  Analysis Date = 03/01/15 
 Pct Recovery = 110%  Analysis Date = 03/01/15 
 Pct Recovery = 110%  Analysis Date = 02/24/15 
 Pct Recovery = 109%  Analysis Date = 02/24/15 
 Pct Recovery = 109%  Analysis Date = 02/20/15 
 Pct Recovery = 109%  Analysis Date = 02/20/15 
 Pct Recovery = 109%  Analysis Date = 02/16/15 
 Pct Recovery = 109%  Analysis Date = 02/16/15 
 Pct Recovery = 109%  Analysis Date = 02/12/15 
 Pct Recovery = 109%  Analysis Date = 02/12/15 
 Pct Recovery = 109%  Analysis Date = 02/08/15 
 Pct Recovery = 108%  Analysis Date = 02/08/15 
 Pct Recovery = 108%  Analysis Date = 02/04/15 
 Pct Recovery = 108%  Analysis Date = 02/04/15 
 Pct Recovery = 108%  Analysis Date = 01/31/15 
 Pct Recovery = 108%  Analysis Date = 01/31/15 
 Pct Recovery = 108%  Analysis Date = 01/26/15 
 Pct Recovery = 107%  Analysis Date = 01/26/15 
 Pct Recovery = 107%  Analysis Date = 01/22/15 
 Pct Recovery = 107%  Analysis Date = 01/22/15 
 Pct Recovery = 107%  Analysis Date = 01/18/15 
 Pct Recovery = 107%  Analysis Date = 01/18/15 
 Pct Recovery = 107%  Analysis Date = 01/14/15 
 Pct Recovery = 106%  Analysis Date = 01/14/15 
 Pct Recovery = 106%  Analysis Date = 01/10/15 
 Pct Recovery = 106%  Analysis Date = 01/10/15 
 Pct Recovery = 106%  Analysis Date = 01/06/15 
 Pct Recovery = 106%  Analysis Date = 01/06/15 
 Pct Recovery = 106%  Analysis Date = 01/02/15 
 Pct Recovery = 106%  Analysis Date = 01/02/15 
 Pct Recovery = 106%  Analysis Date = 12/28/14 
 Pct Recovery = 105%  Analysis Date = 12/28/14 
 Pct Recovery = 105%  Analysis Date = 12/24/14 
 Pct Recovery = 105%  Analysis Date = 12/24/14 
 Pct Recovery = 105%  Analysis Date = 12/20/14 
 Pct Recovery = 105%  Analysis Date = 12/20/14 
 Pct Recovery = 105%  Analysis Date = 12/16/14 
 Pct Recovery = 104%  Analysis Date = 12/16/14 
 Pct Recovery = 104%  Analysis Date = 12/12/14 
 Pct Recovery = 104%  Analysis Date = 12/12/14 
 Pct Recovery = 104%  Analysis Date = 12/08/14 
 Pct Recovery = 104%  Analysis Date = 12/08/14 
 Pct Recovery = 104%  Analysis Date = 12/04/14 
 Pct Recovery = 103%  Analysis Date = 12/04/14 
 Pct Recovery = 103%  Analysis Date = 11/29/14 
 Pct Recovery = 103%  Analysis Date = 11/29/14 
 Pct Recovery = 103%  Analysis Date = 11/25/14 
 Pct Recovery = 103%  Analysis Date = 11/25/14 
 Pct Recovery = 103%  Analysis Date = 11/21/14 
 Pct Recovery = 103%  Analysis Date = 11/21/14 
 Pct Recovery = 103%  Analysis Date = 11/17/14 
 Pct Recovery = 102%  Analysis Date = 11/17/14 
 Pct Recovery = 102%  Analysis Date = 11/13/14 
 Pct Recovery = 102%  Analysis Date = 11/13/14 
 Pct Recovery = 102%  Analysis Date = 11/09/14 
 Pct Recovery = 102%  Analysis Date = 11/09/14 
 Pct Recovery = 102%  Analysis Date = 11/05/14 
 Pct Recovery = 102%  Analysis Date = 11/05/14 
 Pct Recovery = 102%  Analysis Date = 11/01/14 
 Pct Recovery = 101%  Analysis Date = 11/01/14 
 Pct Recovery = 101%  Analysis Date = 10/27/14 
 Pct Recovery = 101%  Analysis Date = 10/27/14 
 Pct Recovery = 101%  Analysis Date = 10/23/14 
 Pct Recovery = 101%  Analysis Date = 10/23/14 
 Pct Recovery = 101%  Analysis Date = 10/19/14 
 Pct Recovery = 100%  Analysis Date = 10/19/14 
 Pct Recovery = 100%  Analysis Date = 10/15/14 
 Pct Recovery = 100%  Analysis Date = 10/15/14 
 Pct Recovery = 100%  Analysis Date = 10/11/14 
 Pct Recovery = 100%  Analysis Date = 10/11/14 
 Pct Recovery = 100%  Analysis Date = 10/07/14 
 Pct Recovery = 100%  Analysis Date = 10/07/14 
 Pct Recovery = 100%  Analysis Date = 10/03/14 
 Pct Recovery = 99%  Analysis Date = 10/03/14 
 Pct Recovery = 99%  Analysis Date = 09/28/14 
 Pct Recovery = 99%  Analysis Date = 09/28/14 
 Pct Recovery = 99%  Analysis Date = 09/24/14 
 Pct Recovery = 99%  Analysis Date = 09/24/14 
 Pct Recovery = 99%  Analysis Date = 09/20/14 
 Pct Recovery = 98%  Analysis Date = 09/20/14 
 Pct Recovery = 98%  Analysis Date = 09/16/14 
 Pct Recovery = 98%  Analysis Date = 09/16/14 
 Pct Recovery = 98%  Analysis Date = 09/12/14 
 Pct Recovery = 98%  Analysis Date = 09/12/14 
 Pct Recovery = 98%  Analysis Date = 09/08/14 
 Pct Recovery = 98%  Analysis Date = 09/08/14 
 Pct Recovery = 98%  Analysis Date = 09/04/14 
 Pct Recovery = 97%  Analysis Date = 09/04/14 
 Pct Recovery = 97%  Analysis Date = 08/30/14 
 Pct Recovery = 97%  Analysis Date = 08/30/14 
 Pct Recovery = 97%  Analysis Date = 08/26/14 
 Pct Recovery = 97%  Analysis Date = 08/26/14 
 Pct Recovery = 97%  Analysis Date = 08/22/14 
 Pct Recovery = 97%  Analysis Date = 08/22/14 
 Pct Recovery = 97%  Analysis Date = 08/18/14 
 Pct Recovery = 96%  Analysis Date = 08/18/14 
 Pct Recovery = 96%  Analysis Date = 08/14/14 
 Pct Recovery = 96%  Analysis Date = 08/14/14 
 Pct Recovery = 96%  Analysis Date = 08/10/14 
 Pct Recovery = 96%  Analysis Date = 08/10/14 
 Pct Recovery = 96%  Analysis Date = 08/06/14 
 Pct Recovery = 96%  Analysis Date = 08/06/14 
 Pct Recovery = 96%  Analysis Date = 08/01/14 
 Pct Recovery = 95%  Analysis Date = 08/01/14 
 Pct Recovery = 95%  Analysis Date = 07/28/14 
 Pct Recovery = 95%  Analysis Date = 07/28/14 
 Pct Recovery = 95%  Analysis Date = 07/24/14 
 Pct Recovery = 95%  Analysis Date = 07/24/14 
 Pct Recovery = 95%  Analysis Date = 07/20/14 
 Pct Recovery = 95%  Analysis Date = 07/20/14 
 Pct Recovery = 95%  Analysis Date = 07/16/14 
 Pct Recovery = 94%  Analysis Date = 07/16/14 
 Pct Recovery = 94%  Analysis Date = 07/12/14 
 Pct Recovery = 94%  Analysis Date = 07/12/14 
 Pct Recovery = 94%  Analysis Date = 07/08/14 
 Pct Recovery = 94%  Analysis Date = 07/08/14 
 Pct Recovery = 94%  Analysis Date = 07/03/14 
 Pct Recovery = 94%  Analysis Date = 07/03/14 
 Pct Recovery = 94%  Analysis Date = 06/29/14 
 Pct Recovery = 94%  Analysis Date = 06/29/14 
 Pct Recovery = 94%  Analysis Date = 06/25/14 
 Pct Recovery = 93%  Analysis Date = 06/25/14 
 Pct Recovery = 93%  Analysis Date = 06/21/14 
 Pct Recovery = 93%  Analysis Date = 06/21/14 
 Pct Recovery = 93%  Analysis Date = 06/17/14 
 Pct Recovery = 93%  Analysis Date = 06/17/14 
 Pct Recovery = 93%  Analysis Date = 06/13/14 
 Pct Recovery = 93%  Analysis Date = 06/13/14 
 Pct Recovery = 93%  Analysis Date = 06/09/14 
 Pct Recovery = 92%  Analysis Date = 06/09/14 
 Pct Recovery = 92%  Analysis Date = 06/04/14 
 Pct Recovery = 92%  Analysis Date = 06/04/14 
 Pct Recovery = 92%  Analysis Date = 05/31/14 
 Pct Recovery = 92%  Analysis Date = 05/31/14 
 Pct Recovery = 92%  Analysis Date = 05/27/14 
 Pct Recovery = 92%  Analysis Date = 05/27/14 
 Pct Recovery = 92%  Analysis Date = 05/23/14 
 Pct Recovery = 91%  Analysis Date = 05/23/14 
 Pct Recovery = 91%  Analysis Date = 05/19/14 
 Pct Recovery = 91%  Analysis Date = 05/19/14 
 Pct Recovery = 91%  Analysis Date = 05/15/14 
 Pct Recovery = 91%  Analysis Date = 05/15/14 
 Pct Recovery = 91%  Analysis Date = 05/11/14 
 Pct Recovery = 91%  Analysis Date = 05/11/14 
 Pct Recovery = 91%  Analysis Date = 05/07/14 
 Pct Recovery = 90%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
CHLOROPICRIN

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 37 107% 21% 99% 25%
Total 37 107% 21% 99% 25%

Sample Statistics
CHLOROPICRIN

Characteristic N % % Basis
Plotted 37 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 37 .  
False Negatives 0 0% 0 out of 37
Not Spiked 18 .  
False Positives 0 0% 0 out of 18

BQS OBSP Determination:
CYCLOHEXANONE
METHOD: 4437 , TESTIDCODE: 77097GM016
Open Data Set

 Analysis Date = 06/29/16 
 SpikeMix = NSI 041516: 40 µl & ChemService 5082800: 40 µl 
 Pct Recovery = 95%  Analysis Date = 07/14/16 
 SpikeMix = NSI 041516: 25 µl & ChemService 5082800: 25 µl & NSI 041416HVOC: 25 µl 
 Pct Recovery = 78%  Analysis Date = 08/11/16 
 SpikeMix = Phenova B20160303: 25 µl & Supelco LC20145V: 25 µl & NSI 041416HVOC: 25 µl 
 Pct Recovery = 91%  Analysis Date = 03/19/15 
 SpikeMix = Supelco LC06437: 20 µl & NSI 031814: 20 µl 
 Pct Recovery = 111%  Analysis Date = 08/20/14 
 SpikeMix = Supelco LC06437: 20 µl & Abs 032014: 20 µl 
 Pct Recovery = 105%  Analysis Date = 06/07/14 
 SpikeMix = ChemService 2615700: 20 µl & Supelco LC06437: 20 µl 
 Pct Recovery = 96%  Analysis Date = 08/13/14 
 SpikeMix = ERA 0321-14-05: 20 µl & Accu 214031128: 20 µl 
 Pct Recovery = 101%  Analysis Date = 07/23/14 
 SpikeMix = Accu 214031128: 20 µl & Abs 032014: 20 µl 
 Pct Recovery = 91%  Analysis Date = 07/11/14 
 SpikeMix = ChemService 2615700: 20 µl & Accu 214031128: 20 µl 
 Pct Recovery = 104%  Analysis Date = 05/07/14 
 SpikeMix = NSI 031814: 20 µl & Accu 214031128: 20 µl 
 Pct Recovery = 85%  Analysis Date = 10/09/15 
 SpikeMix = ERA 0601-15-05: 25 µl & Accu 215041338: 25 µl 
 Pct Recovery = 83%  Analysis Date = 06/26/15 
 SpikeMix = ChemService 3818700: 25 µl & Accu 215041338: 25 µl 
 Pct Recovery = 78%  Analysis Date = 10/09/15 
 SpikeMix = Supelco LC13544: 25 µl & NSI 050515HVOC: 25 µl 
 Pct Recovery = 97%  Analysis Date = 07/27/16 
 SpikeMix = ChemService 5082800: 15 µl & Supelco LC20145V: 15 µl & Accu 216041225: 15 µl 
 Pct Recovery = 87%  Analysis Date = 06/23/16 
 SpikeMix = . 
 Pct Recovery = 77%  Analysis Date = 07/06/16 
 SpikeMix = Phenova B20160303: 15 µl & Accu 216041354: 15 µl & NSI 041416HVOC: 15 µl 
 Pct Recovery = 88%  Analysis Date = 06/03/16 
 SpikeMix = NSI 041516: 15 µl & Phenova B20160303: 15 µl & NSI 041416HVOC: 15 µl 
 Pct Recovery = 98%  Analysis Date = 11/25/15 
 SpikeMix = Accu 215041338: 15 µl & Abs 040315: 15 µl 
 Pct Recovery = 69%  Analysis Date = 09/05/15 
 SpikeMix = Accu 215041338: 15 µl & NSI 050515HVOC: 15 µl 
 Pct Recovery = 71%  Analysis Date = 04/28/16 
 SpikeMix = ChemService 3818700: 15 µl & Supelco LC13544: 15 µl 
 Pct Recovery = 92%  Analysis Date = 08/24/15 
 SpikeMix = ERA 0601-15-05: 15 µl & Supelco LC13544: 15 µl 
 Pct Recovery = 88%  Analysis Date = 07/30/15 
 SpikeMix = Supelco LC13544: 15 µl & NSI 050515HVOC: 15 µl 
 Pct Recovery = 78%  Analysis Date = 05/14/15 
 SpikeMix = ChemService 3818700: 15 µl & Supelco LC13544: 15 µl 
 Pct Recovery = 103%  Analysis Date = 11/22/14 
 SpikeMix = ChemService 2615700: 10 µl & Supelco LC06437: 10 µl 
 Pct Recovery = 93%  Analysis Date = 09/06/14 
 SpikeMix = ERA 0321-14-05: 10 µl & Supelco LC06437: 10 µl 
 Pct Recovery = 120%  Analysis Date = 06/17/14 
 SpikeMix = Supelco LC06437: 10 µl & Abs 032014: 10 µl 
 Pct Recovery = 104%  Analysis Date = 12/13/14 
 SpikeMix = Accu 214031128: 10 µl & NSI 031814: 10 µl 
 Pct Recovery = 88%  Analysis Date = 10/21/14 
 SpikeMix = ERA 0321-14-05A: 10 µl & Accu 214031128: 10 µl 
 Pct Recovery = 80%  Analysis Date = 09/11/14 
 SpikeMix = Accu 214031128: 10 µl & Abs 032014: 10 µl 
 Pct Recovery = 78%  Analysis Date = 05/20/14 
 SpikeMix = ChemService 2615700: 10 µl & Accu 214031128: 10 µl 
 Pct Recovery = 89%  Analysis Date = 02/12/16 
 SpikeMix = ERA 0601-15-05: 10 µl & Accu 215041338: 10 µl 
 Pct Recovery = 84%  Analysis Date = 01/05/16 
 SpikeMix = Accu 215041338: 10 µl & Abs 040315: 10 µl 
 Pct Recovery = 80%  Analysis Date = 05/20/15 
 SpikeMix = ChemService 3818700: 10 µl & Accu 215041338: 10 µl 
 Pct Recovery = 92%  Analysis Date = 03/22/16 
 SpikeMix = Supelco LC13544: 10 µl & NSI 050515HVOC: 10 µl 
 Pct Recovery = 92%  Analysis Date = 12/10/15 
 SpikeMix = ChemService 3818700: 10 µl & Supelco LC13544: 10 µl 
 Pct Recovery = 94%  Analysis Date = 05/05/15 
 SpikeMix = Supelco LC13544: 10 µl & Abs 040315: 10 µl 
 Pct Recovery = 96%  Analysis Date = 08/10/16 
 Pct Recovery = 89%  Analysis Date = 08/06/16 
 Pct Recovery = 89%  Analysis Date = 08/06/16 
 Pct Recovery = 89%  Analysis Date = 08/02/16 
 Pct Recovery = 89%  Analysis Date = 08/02/16 
 Pct Recovery = 89%  Analysis Date = 07/29/16 
 Pct Recovery = 89%  Analysis Date = 07/29/16 
 Pct Recovery = 89%  Analysis Date = 07/25/16 
 Pct Recovery = 89%  Analysis Date = 07/25/16 
 Pct Recovery = 89%  Analysis Date = 07/21/16 
 Pct Recovery = 89%  Analysis Date = 07/21/16 
 Pct Recovery = 89%  Analysis Date = 07/17/16 
 Pct Recovery = 89%  Analysis Date = 07/17/16 
 Pct Recovery = 89%  Analysis Date = 07/13/16 
 Pct Recovery = 88%  Analysis Date = 07/13/16 
 Pct Recovery = 88%  Analysis Date = 07/08/16 
 Pct Recovery = 88%  Analysis Date = 07/08/16 
 Pct Recovery = 88%  Analysis Date = 07/04/16 
 Pct Recovery = 88%  Analysis Date = 07/04/16 
 Pct Recovery = 88%  Analysis Date = 06/30/16 
 Pct Recovery = 88%  Analysis Date = 06/30/16 
 Pct Recovery = 88%  Analysis Date = 06/26/16 
 Pct Recovery = 88%  Analysis Date = 06/26/16 
 Pct Recovery = 88%  Analysis Date = 06/22/16 
 Pct Recovery = 88%  Analysis Date = 06/22/16 
 Pct Recovery = 88%  Analysis Date = 06/18/16 
 Pct Recovery = 88%  Analysis Date = 06/18/16 
 Pct Recovery = 88%  Analysis Date = 06/14/16 
 Pct Recovery = 88%  Analysis Date = 06/14/16 
 Pct Recovery = 88%  Analysis Date = 06/09/16 
 Pct Recovery = 88%  Analysis Date = 06/09/16 
 Pct Recovery = 88%  Analysis Date = 06/05/16 
 Pct Recovery = 88%  Analysis Date = 06/05/16 
 Pct Recovery = 88%  Analysis Date = 06/01/16 
 Pct Recovery = 88%  Analysis Date = 06/01/16 
 Pct Recovery = 88%  Analysis Date = 05/28/16 
 Pct Recovery = 88%  Analysis Date = 05/28/16 
 Pct Recovery = 88%  Analysis Date = 05/24/16 
 Pct Recovery = 88%  Analysis Date = 05/24/16 
 Pct Recovery = 88%  Analysis Date = 05/20/16 
 Pct Recovery = 88%  Analysis Date = 05/20/16 
 Pct Recovery = 88%  Analysis Date = 05/16/16 
 Pct Recovery = 87%  Analysis Date = 05/16/16 
 Pct Recovery = 87%  Analysis Date = 05/12/16 
 Pct Recovery = 87%  Analysis Date = 05/12/16 
 Pct Recovery = 87%  Analysis Date = 05/07/16 
 Pct Recovery = 87%  Analysis Date = 05/07/16 
 Pct Recovery = 87%  Analysis Date = 05/03/16 
 Pct Recovery = 87%  Analysis Date = 05/03/16 
 Pct Recovery = 87%  Analysis Date = 04/29/16 
 Pct Recovery = 87%  Analysis Date = 04/29/16 
 Pct Recovery = 87%  Analysis Date = 04/25/16 
 Pct Recovery = 87%  Analysis Date = 04/25/16 
 Pct Recovery = 87%  Analysis Date = 04/21/16 
 Pct Recovery = 87%  Analysis Date = 04/21/16 
 Pct Recovery = 87%  Analysis Date = 04/17/16 
 Pct Recovery = 87%  Analysis Date = 04/17/16 
 Pct Recovery = 87%  Analysis Date = 04/13/16 
 Pct Recovery = 87%  Analysis Date = 04/13/16 
 Pct Recovery = 87%  Analysis Date = 04/08/16 
 Pct Recovery = 87%  Analysis Date = 04/08/16 
 Pct Recovery = 87%  Analysis Date = 04/04/16 
 Pct Recovery = 87%  Analysis Date = 04/04/16 
 Pct Recovery = 87%  Analysis Date = 03/31/16 
 Pct Recovery = 87%  Analysis Date = 03/31/16 
 Pct Recovery = 87%  Analysis Date = 03/27/16 
 Pct Recovery = 87%  Analysis Date = 03/27/16 
 Pct Recovery = 87%  Analysis Date = 03/23/16 
 Pct Recovery = 87%  Analysis Date = 03/23/16 
 Pct Recovery = 87%  Analysis Date = 03/19/16 
 Pct Recovery = 86%  Analysis Date = 03/19/16 
 Pct Recovery = 86%  Analysis Date = 03/15/16 
 Pct Recovery = 86%  Analysis Date = 03/15/16 
 Pct Recovery = 86%  Analysis Date = 03/11/16 
 Pct Recovery = 86%  Analysis Date = 03/11/16 
 Pct Recovery = 86%  Analysis Date = 03/06/16 
 Pct Recovery = 86%  Analysis Date = 03/06/16 
 Pct Recovery = 86%  Analysis Date = 03/02/16 
 Pct Recovery = 86%  Analysis Date = 03/02/16 
 Pct Recovery = 86%  Analysis Date = 02/27/16 
 Pct Recovery = 86%  Analysis Date = 02/27/16 
 Pct Recovery = 86%  Analysis Date = 02/23/16 
 Pct Recovery = 86%  Analysis Date = 02/23/16 
 Pct Recovery = 86%  Analysis Date = 02/19/16 
 Pct Recovery = 86%  Analysis Date = 02/19/16 
 Pct Recovery = 86%  Analysis Date = 02/15/16 
 Pct Recovery = 86%  Analysis Date = 02/15/16 
 Pct Recovery = 86%  Analysis Date = 02/11/16 
 Pct Recovery = 86%  Analysis Date = 02/11/16 
 Pct Recovery = 86%  Analysis Date = 02/06/16 
 Pct Recovery = 86%  Analysis Date = 02/06/16 
 Pct Recovery = 86%  Analysis Date = 02/02/16 
 Pct Recovery = 86%  Analysis Date = 02/02/16 
 Pct Recovery = 86%  Analysis Date = 01/29/16 
 Pct Recovery = 86%  Analysis Date = 01/29/16 
 Pct Recovery = 86%  Analysis Date = 01/25/16 
 Pct Recovery = 86%  Analysis Date = 01/25/16 
 Pct Recovery = 86%  Analysis Date = 01/21/16 
 Pct Recovery = 86%  Analysis Date = 01/21/16 
 Pct Recovery = 86%  Analysis Date = 01/17/16 
 Pct Recovery = 86%  Analysis Date = 01/17/16 
 Pct Recovery = 86%  Analysis Date = 01/13/16 
 Pct Recovery = 86%  Analysis Date = 01/13/16 
 Pct Recovery = 86%  Analysis Date = 01/08/16 
 Pct Recovery = 86%  Analysis Date = 01/08/16 
 Pct Recovery = 86%  Analysis Date = 01/04/16 
 Pct Recovery = 86%  Analysis Date = 01/04/16 
 Pct Recovery = 86%  Analysis Date = 12/31/15 
 Pct Recovery = 86%  Analysis Date = 12/31/15 
 Pct Recovery = 86%  Analysis Date = 12/27/15 
 Pct Recovery = 86%  Analysis Date = 12/27/15 
 Pct Recovery = 86%  Analysis Date = 12/23/15 
 Pct Recovery = 86%  Analysis Date = 12/23/15 
 Pct Recovery = 86%  Analysis Date = 12/19/15 
 Pct Recovery = 86%  Analysis Date = 12/19/15 
 Pct Recovery = 86%  Analysis Date = 12/15/15 
 Pct Recovery = 86%  Analysis Date = 12/15/15 
 Pct Recovery = 86%  Analysis Date = 12/11/15 
 Pct Recovery = 86%  Analysis Date = 12/11/15 
 Pct Recovery = 86%  Analysis Date = 12/06/15 
 Pct Recovery = 86%  Analysis Date = 12/06/15 
 Pct Recovery = 86%  Analysis Date = 12/02/15 
 Pct Recovery = 86%  Analysis Date = 12/02/15 
 Pct Recovery = 86%  Analysis Date = 11/28/15 
 Pct Recovery = 85%  Analysis Date = 11/28/15 
 Pct Recovery = 85%  Analysis Date = 11/24/15 
 Pct Recovery = 85%  Analysis Date = 11/24/15 
 Pct Recovery = 85%  Analysis Date = 11/20/15 
 Pct Recovery = 85%  Analysis Date = 11/20/15 
 Pct Recovery = 85%  Analysis Date = 11/16/15 
 Pct Recovery = 85%  Analysis Date = 11/16/15 
 Pct Recovery = 85%  Analysis Date = 11/12/15 
 Pct Recovery = 85%  Analysis Date = 11/12/15 
 Pct Recovery = 85%  Analysis Date = 11/07/15 
 Pct Recovery = 85%  Analysis Date = 11/07/15 
 Pct Recovery = 85%  Analysis Date = 11/03/15 
 Pct Recovery = 85%  Analysis Date = 11/03/15 
 Pct Recovery = 85%  Analysis Date = 10/30/15 
 Pct Recovery = 85%  Analysis Date = 10/30/15 
 Pct Recovery = 85%  Analysis Date = 10/26/15 
 Pct Recovery = 85%  Analysis Date = 10/26/15 
 Pct Recovery = 85%  Analysis Date = 10/22/15 
 Pct Recovery = 85%  Analysis Date = 10/22/15 
 Pct Recovery = 85%  Analysis Date = 10/18/15 
 Pct Recovery = 85%  Analysis Date = 10/18/15 
 Pct Recovery = 85%  Analysis Date = 10/14/15 
 Pct Recovery = 85%  Analysis Date = 10/14/15 
 Pct Recovery = 85%  Analysis Date = 10/10/15 
 Pct Recovery = 85%  Analysis Date = 10/10/15 
 Pct Recovery = 85%  Analysis Date = 10/05/15 
 Pct Recovery = 85%  Analysis Date = 10/05/15 
 Pct Recovery = 85%  Analysis Date = 10/01/15 
 Pct Recovery = 86%  Analysis Date = 10/01/15 
 Pct Recovery = 86%  Analysis Date = 09/27/15 
 Pct Recovery = 86%  Analysis Date = 09/27/15 
 Pct Recovery = 86%  Analysis Date = 09/23/15 
 Pct Recovery = 86%  Analysis Date = 09/23/15 
 Pct Recovery = 86%  Analysis Date = 09/19/15 
 Pct Recovery = 86%  Analysis Date = 09/19/15 
 Pct Recovery = 86%  Analysis Date = 09/15/15 
 Pct Recovery = 86%  Analysis Date = 09/15/15 
 Pct Recovery = 86%  Analysis Date = 09/11/15 
 Pct Recovery = 86%  Analysis Date = 09/11/15 
 Pct Recovery = 86%  Analysis Date = 09/06/15 
 Pct Recovery = 87%  Analysis Date = 09/06/15 
 Pct Recovery = 87%  Analysis Date = 09/02/15 
 Pct Recovery = 87%  Analysis Date = 09/02/15 
 Pct Recovery = 87%  Analysis Date = 08/29/15 
 Pct Recovery = 87%  Analysis Date = 08/29/15 
 Pct Recovery = 87%  Analysis Date = 08/25/15 
 Pct Recovery = 87%  Analysis Date = 08/25/15 
 Pct Recovery = 87%  Analysis Date = 08/21/15 
 Pct Recovery = 87%  Analysis Date = 08/21/15 
 Pct Recovery = 87%  Analysis Date = 08/17/15 
 Pct Recovery = 87%  Analysis Date = 08/17/15 
 Pct Recovery = 87%  Analysis Date = 08/13/15 
 Pct Recovery = 87%  Analysis Date = 08/13/15 
 Pct Recovery = 87%  Analysis Date = 08/08/15 
 Pct Recovery = 88%  Analysis Date = 08/08/15 
 Pct Recovery = 88%  Analysis Date = 08/04/15 
 Pct Recovery = 88%  Analysis Date = 08/04/15 
 Pct Recovery = 88%  Analysis Date = 07/31/15 
 Pct Recovery = 88%  Analysis Date = 07/31/15 
 Pct Recovery = 88%  Analysis Date = 07/27/15 
 Pct Recovery = 88%  Analysis Date = 07/27/15 
 Pct Recovery = 88%  Analysis Date = 07/23/15 
 Pct Recovery = 88%  Analysis Date = 07/23/15 
 Pct Recovery = 88%  Analysis Date = 07/19/15 
 Pct Recovery = 88%  Analysis Date = 07/19/15 
 Pct Recovery = 88%  Analysis Date = 07/15/15 
 Pct Recovery = 89%  Analysis Date = 07/15/15 
 Pct Recovery = 89%  Analysis Date = 07/11/15 
 Pct Recovery = 89%  Analysis Date = 07/11/15 
 Pct Recovery = 89%  Analysis Date = 07/06/15 
 Pct Recovery = 89%  Analysis Date = 07/06/15 
 Pct Recovery = 89%  Analysis Date = 07/02/15 
 Pct Recovery = 89%  Analysis Date = 07/02/15 
 Pct Recovery = 89%  Analysis Date = 06/28/15 
 Pct Recovery = 89%  Analysis Date = 06/28/15 
 Pct Recovery = 89%  Analysis Date = 06/24/15 
 Pct Recovery = 89%  Analysis Date = 06/24/15 
 Pct Recovery = 89%  Analysis Date = 06/20/15 
 Pct Recovery = 89%  Analysis Date = 06/20/15 
 Pct Recovery = 89%  Analysis Date = 06/16/15 
 Pct Recovery = 89%  Analysis Date = 06/16/15 
 Pct Recovery = 89%  Analysis Date = 06/12/15 
 Pct Recovery = 90%  Analysis Date = 06/12/15 
 Pct Recovery = 90%  Analysis Date = 06/07/15 
 Pct Recovery = 90%  Analysis Date = 06/07/15 
 Pct Recovery = 90%  Analysis Date = 06/03/15 
 Pct Recovery = 90%  Analysis Date = 06/03/15 
 Pct Recovery = 90%  Analysis Date = 05/30/15 
 Pct Recovery = 90%  Analysis Date = 05/30/15 
 Pct Recovery = 90%  Analysis Date = 05/26/15 
 Pct Recovery = 90%  Analysis Date = 05/26/15 
 Pct Recovery = 90%  Analysis Date = 05/22/15 
 Pct Recovery = 90%  Analysis Date = 05/22/15 
 Pct Recovery = 90%  Analysis Date = 05/18/15 
 Pct Recovery = 90%  Analysis Date = 05/18/15 
 Pct Recovery = 90%  Analysis Date = 05/14/15 
 Pct Recovery = 90%  Analysis Date = 05/14/15 
 Pct Recovery = 90%  Analysis Date = 05/10/15 
 Pct Recovery = 91%  Analysis Date = 05/10/15 
 Pct Recovery = 91%  Analysis Date = 05/05/15 
 Pct Recovery = 91%  Analysis Date = 05/05/15 
 Pct Recovery = 91%  Analysis Date = 05/01/15 
 Pct Recovery = 91%  Analysis Date = 05/01/15 
 Pct Recovery = 91%  Analysis Date = 04/27/15 
 Pct Recovery = 91%  Analysis Date = 04/27/15 
 Pct Recovery = 91%  Analysis Date = 04/23/15 
 Pct Recovery = 91%  Analysis Date = 04/23/15 
 Pct Recovery = 91%  Analysis Date = 04/19/15 
 Pct Recovery = 91%  Analysis Date = 04/19/15 
 Pct Recovery = 91%  Analysis Date = 04/15/15 
 Pct Recovery = 91%  Analysis Date = 04/15/15 
 Pct Recovery = 91%  Analysis Date = 04/11/15 
 Pct Recovery = 91%  Analysis Date = 04/11/15 
 Pct Recovery = 91%  Analysis Date = 04/06/15 
 Pct Recovery = 92%  Analysis Date = 04/06/15 
 Pct Recovery = 92%  Analysis Date = 04/02/15 
 Pct Recovery = 92%  Analysis Date = 04/02/15 
 Pct Recovery = 92%  Analysis Date = 03/29/15 
 Pct Recovery = 92%  Analysis Date = 03/29/15 
 Pct Recovery = 92%  Analysis Date = 03/25/15 
 Pct Recovery = 92%  Analysis Date = 03/25/15 
 Pct Recovery = 92%  Analysis Date = 03/21/15 
 Pct Recovery = 92%  Analysis Date = 03/21/15 
 Pct Recovery = 92%  Analysis Date = 03/17/15 
 Pct Recovery = 92%  Analysis Date = 03/17/15 
 Pct Recovery = 92%  Analysis Date = 03/13/15 
 Pct Recovery = 92%  Analysis Date = 03/13/15 
 Pct Recovery = 92%  Analysis Date = 03/08/15 
 Pct Recovery = 92%  Analysis Date = 03/08/15 
 Pct Recovery = 92%  Analysis Date = 03/04/15 
 Pct Recovery = 93%  Analysis Date = 03/04/15 
 Pct Recovery = 93%  Analysis Date = 02/28/15 
 Pct Recovery = 93%  Analysis Date = 02/28/15 
 Pct Recovery = 93%  Analysis Date = 02/24/15 
 Pct Recovery = 93%  Analysis Date = 02/24/15 
 Pct Recovery = 93%  Analysis Date = 02/20/15 
 Pct Recovery = 93%  Analysis Date = 02/20/15 
 Pct Recovery = 93%  Analysis Date = 02/16/15 
 Pct Recovery = 93%  Analysis Date = 02/16/15 
 Pct Recovery = 93%  Analysis Date = 02/12/15 
 Pct Recovery = 93%  Analysis Date = 02/12/15 
 Pct Recovery = 93%  Analysis Date = 02/08/15 
 Pct Recovery = 93%  Analysis Date = 02/08/15 
 Pct Recovery = 93%  Analysis Date = 02/03/15 
 Pct Recovery = 94%  Analysis Date = 02/03/15 
 Pct Recovery = 94%  Analysis Date = 01/30/15 
 Pct Recovery = 94%  Analysis Date = 01/30/15 
 Pct Recovery = 94%  Analysis Date = 01/26/15 
 Pct Recovery = 94%  Analysis Date = 01/26/15 
 Pct Recovery = 94%  Analysis Date = 01/22/15 
 Pct Recovery = 94%  Analysis Date = 01/22/15 
 Pct Recovery = 94%  Analysis Date = 01/18/15 
 Pct Recovery = 94%  Analysis Date = 01/18/15 
 Pct Recovery = 94%  Analysis Date = 01/14/15 
 Pct Recovery = 94%  Analysis Date = 01/14/15 
 Pct Recovery = 94%  Analysis Date = 01/10/15 
 Pct Recovery = 94%  Analysis Date = 01/10/15 
 Pct Recovery = 94%  Analysis Date = 01/05/15 
 Pct Recovery = 94%  Analysis Date = 01/05/15 
 Pct Recovery = 94%  Analysis Date = 01/01/15 
 Pct Recovery = 95%  Analysis Date = 01/01/15 
 Pct Recovery = 95%  Analysis Date = 12/28/14 
 Pct Recovery = 95%  Analysis Date = 12/28/14 
 Pct Recovery = 95%  Analysis Date = 12/24/14 
 Pct Recovery = 95%  Analysis Date = 12/24/14 
 Pct Recovery = 95%  Analysis Date = 12/20/14 
 Pct Recovery = 95%  Analysis Date = 12/20/14 
 Pct Recovery = 95%  Analysis Date = 12/16/14 
 Pct Recovery = 95%  Analysis Date = 12/16/14 
 Pct Recovery = 95%  Analysis Date = 12/12/14 
 Pct Recovery = 95%  Analysis Date = 12/12/14 
 Pct Recovery = 95%  Analysis Date = 12/08/14 
 Pct Recovery = 95%  Analysis Date = 12/08/14 
 Pct Recovery = 95%  Analysis Date = 12/03/14 
 Pct Recovery = 96%  Analysis Date = 12/03/14 
 Pct Recovery = 96%  Analysis Date = 11/29/14 
 Pct Recovery = 96%  Analysis Date = 11/29/14 
 Pct Recovery = 96%  Analysis Date = 11/25/14 
 Pct Recovery = 96%  Analysis Date = 11/25/14 
 Pct Recovery = 96%  Analysis Date = 11/21/14 
 Pct Recovery = 96%  Analysis Date = 11/21/14 
 Pct Recovery = 96%  Analysis Date = 11/17/14 
 Pct Recovery = 96%  Analysis Date = 11/17/14 
 Pct Recovery = 96%  Analysis Date = 11/13/14 
 Pct Recovery = 96%  Analysis Date = 11/13/14 
 Pct Recovery = 96%  Analysis Date = 11/09/14 
 Pct Recovery = 96%  Analysis Date = 11/09/14 
 Pct Recovery = 96%  Analysis Date = 11/04/14 
 Pct Recovery = 96%  Analysis Date = 11/04/14 
 Pct Recovery = 96%  Analysis Date = 10/31/14 
 Pct Recovery = 96%  Analysis Date = 10/31/14 
 Pct Recovery = 96%  Analysis Date = 10/27/14 
 Pct Recovery = 96%  Analysis Date = 10/27/14 
 Pct Recovery = 96%  Analysis Date = 10/23/14 
 Pct Recovery = 96%  Analysis Date = 10/23/14 
 Pct Recovery = 96%  Analysis Date = 10/19/14 
 Pct Recovery = 96%  Analysis Date = 10/19/14 
 Pct Recovery = 96%  Analysis Date = 10/15/14 
 Pct Recovery = 96%  Analysis Date = 10/15/14 
 Pct Recovery = 96%  Analysis Date = 10/11/14 
 Pct Recovery = 96%  Analysis Date = 10/11/14 
 Pct Recovery = 96%  Analysis Date = 10/06/14 
 Pct Recovery = 96%  Analysis Date = 10/06/14 
 Pct Recovery = 96%  Analysis Date = 10/02/14 
 Pct Recovery = 96%  Analysis Date = 10/02/14 
 Pct Recovery = 96%  Analysis Date = 09/28/14 
 Pct Recovery = 96%  Analysis Date = 09/28/14 
 Pct Recovery = 96%  Analysis Date = 09/24/14 
 Pct Recovery = 96%  Analysis Date = 09/24/14 
 Pct Recovery = 96%  Analysis Date = 09/20/14 
 Pct Recovery = 96%  Analysis Date = 09/20/14 
 Pct Recovery = 96%  Analysis Date = 09/16/14 
 Pct Recovery = 96%  Analysis Date = 09/16/14 
 Pct Recovery = 96%  Analysis Date = 09/12/14 
 Pct Recovery = 96%  Analysis Date = 09/12/14 
 Pct Recovery = 96%  Analysis Date = 09/08/14 
 Pct Recovery = 96%  Analysis Date = 09/08/14 
 Pct Recovery = 96%  Analysis Date = 09/03/14 
 Pct Recovery = 96%  Analysis Date = 09/03/14 
 Pct Recovery = 96%  Analysis Date = 08/30/14 
 Pct Recovery = 96%  Analysis Date = 08/30/14 
 Pct Recovery = 96%  Analysis Date = 08/26/14 
 Pct Recovery = 96%  Analysis Date = 08/26/14 
 Pct Recovery = 96%  Analysis Date = 08/22/14 
 Pct Recovery = 96%  Analysis Date = 08/22/14 
 Pct Recovery = 96%  Analysis Date = 08/18/14 
 Pct Recovery = 96%  Analysis Date = 08/18/14 
 Pct Recovery = 96%  Analysis Date = 08/14/14 
 Pct Recovery = 96%  Analysis Date = 08/14/14 
 Pct Recovery = 96%  Analysis Date = 08/10/14 
 Pct Recovery = 96%  Analysis Date = 08/10/14 
 Pct Recovery = 96%  Analysis Date = 08/05/14 
 Pct Recovery = 96%  Analysis Date = 08/05/14 
 Pct Recovery = 96%  Analysis Date = 08/01/14 
 Pct Recovery = 96%  Analysis Date = 08/01/14 
 Pct Recovery = 96%  Analysis Date = 07/28/14 
 Pct Recovery = 96%  Analysis Date = 07/28/14 
 Pct Recovery = 96%  Analysis Date = 07/24/14 
 Pct Recovery = 96%  Analysis Date = 07/24/14 
 Pct Recovery = 96%  Analysis Date = 07/20/14 
 Pct Recovery = 96%  Analysis Date = 07/20/14 
 Pct Recovery = 96%  Analysis Date = 07/16/14 
 Pct Recovery = 96%  Analysis Date = 07/16/14 
 Pct Recovery = 96%  Analysis Date = 07/12/14 
 Pct Recovery = 95%  Analysis Date = 07/12/14 
 Pct Recovery = 95%  Analysis Date = 07/08/14 
 Pct Recovery = 95%  Analysis Date = 07/08/14 
 Pct Recovery = 95%  Analysis Date = 07/03/14 
 Pct Recovery = 95%  Analysis Date = 07/03/14 
 Pct Recovery = 95%  Analysis Date = 06/29/14 
 Pct Recovery = 95%  Analysis Date = 06/29/14 
 Pct Recovery = 95%  Analysis Date = 06/25/14 
 Pct Recovery = 95%  Analysis Date = 06/25/14 
 Pct Recovery = 95%  Analysis Date = 06/21/14 
 Pct Recovery = 95%  Analysis Date = 06/21/14 
 Pct Recovery = 95%  Analysis Date = 06/17/14 
 Pct Recovery = 95%  Analysis Date = 06/17/14 
 Pct Recovery = 95%  Analysis Date = 06/13/14 
 Pct Recovery = 95%  Analysis Date = 06/13/14 
 Pct Recovery = 95%  Analysis Date = 06/09/14 
 Pct Recovery = 95%  Analysis Date = 06/09/14 
 Pct Recovery = 95%  Analysis Date = 06/04/14 
 Pct Recovery = 95%  Analysis Date = 06/04/14 
 Pct Recovery = 95%  Analysis Date = 05/31/14 
 Pct Recovery = 95%  Analysis Date = 05/31/14 
 Pct Recovery = 95%  Analysis Date = 05/27/14 
 Pct Recovery = 95%  Analysis Date = 05/27/14 
 Pct Recovery = 95%  Analysis Date = 05/23/14 
 Pct Recovery = 95%  Analysis Date = 05/23/14 
 Pct Recovery = 95%  Analysis Date = 05/19/14 
 Pct Recovery = 95%  Analysis Date = 05/19/14 
 Pct Recovery = 95%  Analysis Date = 05/15/14 
 Pct Recovery = 95%  Analysis Date = 05/15/14 
 Pct Recovery = 95%  Analysis Date = 05/11/14 
 Pct Recovery = 95%  Analysis Date = 05/11/14 
 Pct Recovery = 95%  Analysis Date = 05/07/14 
 Pct Recovery = 95%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
CYCLOHEXANONE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 36 90% 11% 91% 11%
Total 36 90% 11% 91% 11%

Sample Statistics
CYCLOHEXANONE

Characteristic N % % Basis
Plotted 36 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 36 .  
False Negatives 0 0% 0 out of 36
Not Spiked 19 .  
False Positives 0 0% 0 out of 19

BQS OBSP Determination:
DIETHYLAMINE, N-NITROSO-
METHOD: 4437 , TESTIDCODE: 78200GM016
Open Data Set

 Analysis Date = 06/29/16 
 SpikeMix = NSI 041516: 40 µl & ChemService 5082800: 40 µl 
 Pct Recovery = 82%  Analysis Date = 07/14/16 
 SpikeMix = NSI 041516: 25 µl & ChemService 5082800: 25 µl & NSI 041416HVOC: 25 µl 
 Pct Recovery = 86%  Analysis Date = 08/11/16 
 SpikeMix = Phenova B20160303: 25 µl & Supelco LC20145V: 25 µl & NSI 041416HVOC: 25 µl 
 Pct Recovery = 79%  Analysis Date = 01/22/16 
 SpikeMix = NSI 050515HVOC: 25 µl & ERA 0601-15-05: 25 µl 
 Pct Recovery = 79%  Analysis Date = 10/09/15 
 SpikeMix = Supelco LC13544: 25 µl & NSI 050515HVOC: 25 µl 
 Pct Recovery = 94%  Analysis Date = 06/25/15 
 SpikeMix = ChemService 3818700: 25 µl & NSI 050515HVOC: 25 µl 
 Pct Recovery = 77%  Analysis Date = 07/27/16 
 SpikeMix = ChemService 5082800: 15 µl & Supelco LC20145V: 15 µl & Accu 216041225: 15 µl 
 Pct Recovery = 72%  Analysis Date = 06/23/16 
 SpikeMix = . 
 Pct Recovery = 63%  Analysis Date = 07/06/16 
 SpikeMix = Phenova B20160303: 15 µl & Accu 216041354: 15 µl & NSI 041416HVOC: 15 µl 
 Pct Recovery = 94%  Analysis Date = 06/03/16 
 SpikeMix = NSI 041516: 15 µl & Phenova B20160303: 15 µl & NSI 041416HVOC: 15 µl 
 Pct Recovery = 88%  Analysis Date = 01/10/15 
 SpikeMix = Abs 032014: 20 µl & ERA 0321-14-05A: 20 µl 
 Pct Recovery = 103%  Analysis Date = 08/13/14 
 SpikeMix = ERA 0321-14-05: 20 µl & Accu 214031128: 20 µl 
 Pct Recovery = 97%  Analysis Date = 07/11/14 
 SpikeMix = ChemService 2615700: 20 µl & Accu 214031128: 20 µl 
 Pct Recovery = 99%  Analysis Date = 07/03/14 
 SpikeMix = Abs 032014: 20 µl & ChemService 2615700: 20 µl 
 Pct Recovery = 99%  Analysis Date = 06/07/14 
 SpikeMix = ChemService 2615700: 20 µl & Supelco LC06437: 20 µl 
 Pct Recovery = 95%  Analysis Date = 06/06/14 
 SpikeMix = NSI 031814: 20 µl & ChemService 2615700: 20 µl 
 Pct Recovery = 99%  Analysis Date = 09/05/15 
 SpikeMix = Accu 215041338: 15 µl & NSI 050515HVOC: 15 µl 
 Pct Recovery = 72%  Analysis Date = 07/30/15 
 SpikeMix = Supelco LC13544: 15 µl & NSI 050515HVOC: 15 µl 
 Pct Recovery = 77%  Analysis Date = 06/16/15 
 SpikeMix = ChemService 3818700: 15 µl & NSI 050515HVOC: 15 µl 
 Pct Recovery = 63%  Analysis Date = 11/25/15 
 SpikeMix = Accu 215041338: 15 µl & Abs 040315: 15 µl 
 Pct Recovery = 87%  Analysis Date = 09/24/15 
 SpikeMix = Abs 040315: 15 µl & ERA 0601-15-05: 15 µl 
 Pct Recovery = 87%  Analysis Date = 03/22/16 
 SpikeMix = Supelco LC13544: 10 µl & NSI 050515HVOC: 10 µl 
 Pct Recovery = 96%  Analysis Date = 12/05/15 
 SpikeMix = NSI 050515HVOC: 10 µl & ERA 0601-15-05: 10 µl 
 Pct Recovery = 74%  Analysis Date = 04/09/16 
 SpikeMix = Abs 040315: 10 µl & ChemService 3818700: 10 µl 
 Pct Recovery = 81%  Analysis Date = 01/05/16 
 SpikeMix = Accu 215041338: 10 µl & Abs 040315: 10 µl 
 Pct Recovery = 97%  Analysis Date = 10/23/15 
 SpikeMix = Abs 040315: 10 µl & ChemService 3818700: 10 µl 
 Pct Recovery = 95%  Analysis Date = 08/14/15 
 SpikeMix = Abs 040315: 10 µl & ERA 0601-15-05: 10 µl 
 Pct Recovery = 69%  Analysis Date = 05/05/15 
 SpikeMix = Supelco LC13544: 10 µl & Abs 040315: 10 µl 
 Pct Recovery = 108%  Analysis Date = 04/25/15 
 SpikeMix = Abs 032014: 10 µl & ERA 0321-14-05A: 10 µl 
 Pct Recovery = 101%  Analysis Date = 10/21/14 
 SpikeMix = ERA 0321-14-05A: 10 µl & Accu 214031128: 10 µl 
 Pct Recovery = 111%  Analysis Date = 09/06/14 
 SpikeMix = ERA 0321-14-05: 10 µl & Supelco LC06437: 10 µl 
 Pct Recovery = 135%  Analysis Date = 11/22/14 
 SpikeMix = ChemService 2615700: 10 µl & Supelco LC06437: 10 µl 
 Pct Recovery = 89%  Analysis Date = 07/30/14 
 SpikeMix = NSI 031814: 10 µl & ChemService 2615700: 10 µl 
 Pct Recovery = 105%  Analysis Date = 05/20/14 
 SpikeMix = ChemService 2615700: 10 µl & Accu 214031128: 10 µl 
 Pct Recovery = 131%  Analysis Date = 08/10/16 
 Pct Recovery = 80%  Analysis Date = 08/06/16 
 Pct Recovery = 80%  Analysis Date = 08/06/16 
 Pct Recovery = 80%  Analysis Date = 08/02/16 
 Pct Recovery = 80%  Analysis Date = 08/02/16 
 Pct Recovery = 80%  Analysis Date = 07/29/16 
 Pct Recovery = 80%  Analysis Date = 07/29/16 
 Pct Recovery = 80%  Analysis Date = 07/25/16 
 Pct Recovery = 81%  Analysis Date = 07/25/16 
 Pct Recovery = 81%  Analysis Date = 07/21/16 
 Pct Recovery = 81%  Analysis Date = 07/21/16 
 Pct Recovery = 81%  Analysis Date = 07/17/16 
 Pct Recovery = 81%  Analysis Date = 07/17/16 
 Pct Recovery = 81%  Analysis Date = 07/13/16 
 Pct Recovery = 81%  Analysis Date = 07/13/16 
 Pct Recovery = 81%  Analysis Date = 07/09/16 
 Pct Recovery = 81%  Analysis Date = 07/09/16 
 Pct Recovery = 81%  Analysis Date = 07/05/16 
 Pct Recovery = 81%  Analysis Date = 07/05/16 
 Pct Recovery = 81%  Analysis Date = 07/01/16 
 Pct Recovery = 81%  Analysis Date = 07/01/16 
 Pct Recovery = 81%  Analysis Date = 06/27/16 
 Pct Recovery = 81%  Analysis Date = 06/27/16 
 Pct Recovery = 81%  Analysis Date = 06/23/16 
 Pct Recovery = 82%  Analysis Date = 06/23/16 
 Pct Recovery = 82%  Analysis Date = 06/19/16 
 Pct Recovery = 82%  Analysis Date = 06/19/16 
 Pct Recovery = 82%  Analysis Date = 06/15/16 
 Pct Recovery = 82%  Analysis Date = 06/15/16 
 Pct Recovery = 82%  Analysis Date = 06/10/16 
 Pct Recovery = 82%  Analysis Date = 06/10/16 
 Pct Recovery = 82%  Analysis Date = 06/06/16 
 Pct Recovery = 82%  Analysis Date = 06/06/16 
 Pct Recovery = 82%  Analysis Date = 06/02/16 
 Pct Recovery = 82%  Analysis Date = 06/02/16 
 Pct Recovery = 82%  Analysis Date = 05/29/16 
 Pct Recovery = 82%  Analysis Date = 05/29/16 
 Pct Recovery = 82%  Analysis Date = 05/25/16 
 Pct Recovery = 82%  Analysis Date = 05/25/16 
 Pct Recovery = 82%  Analysis Date = 05/21/16 
 Pct Recovery = 82%  Analysis Date = 05/21/16 
 Pct Recovery = 82%  Analysis Date = 05/17/16 
 Pct Recovery = 82%  Analysis Date = 05/17/16 
 Pct Recovery = 82%  Analysis Date = 05/13/16 
 Pct Recovery = 83%  Analysis Date = 05/13/16 
 Pct Recovery = 83%  Analysis Date = 05/09/16 
 Pct Recovery = 83%  Analysis Date = 05/09/16 
 Pct Recovery = 83%  Analysis Date = 05/05/16 
 Pct Recovery = 83%  Analysis Date = 05/05/16 
 Pct Recovery = 83%  Analysis Date = 05/01/16 
 Pct Recovery = 83%  Analysis Date = 05/01/16 
 Pct Recovery = 83%  Analysis Date = 04/27/16 
 Pct Recovery = 83%  Analysis Date = 04/27/16 
 Pct Recovery = 83%  Analysis Date = 04/23/16 
 Pct Recovery = 83%  Analysis Date = 04/23/16 
 Pct Recovery = 83%  Analysis Date = 04/19/16 
 Pct Recovery = 83%  Analysis Date = 04/19/16 
 Pct Recovery = 83%  Analysis Date = 04/14/16 
 Pct Recovery = 83%  Analysis Date = 04/14/16 
 Pct Recovery = 83%  Analysis Date = 04/10/16 
 Pct Recovery = 83%  Analysis Date = 04/10/16 
 Pct Recovery = 83%  Analysis Date = 04/06/16 
 Pct Recovery = 84%  Analysis Date = 04/06/16 
 Pct Recovery = 84%  Analysis Date = 04/02/16 
 Pct Recovery = 84%  Analysis Date = 04/02/16 
 Pct Recovery = 84%  Analysis Date = 03/29/16 
 Pct Recovery = 84%  Analysis Date = 03/29/16 
 Pct Recovery = 84%  Analysis Date = 03/25/16 
 Pct Recovery = 84%  Analysis Date = 03/25/16 
 Pct Recovery = 84%  Analysis Date = 03/21/16 
 Pct Recovery = 84%  Analysis Date = 03/21/16 
 Pct Recovery = 84%  Analysis Date = 03/17/16 
 Pct Recovery = 84%  Analysis Date = 03/17/16 
 Pct Recovery = 84%  Analysis Date = 03/13/16 
 Pct Recovery = 84%  Analysis Date = 03/13/16 
 Pct Recovery = 84%  Analysis Date = 03/09/16 
 Pct Recovery = 84%  Analysis Date = 03/09/16 
 Pct Recovery = 84%  Analysis Date = 03/05/16 
 Pct Recovery = 84%  Analysis Date = 03/05/16 
 Pct Recovery = 84%  Analysis Date = 03/01/16 
 Pct Recovery = 84%  Analysis Date = 03/01/16 
 Pct Recovery = 84%  Analysis Date = 02/26/16 
 Pct Recovery = 84%  Analysis Date = 02/26/16 
 Pct Recovery = 84%  Analysis Date = 02/22/16 
 Pct Recovery = 84%  Analysis Date = 02/22/16 
 Pct Recovery = 84%  Analysis Date = 02/17/16 
 Pct Recovery = 84%  Analysis Date = 02/17/16 
 Pct Recovery = 84%  Analysis Date = 02/13/16 
 Pct Recovery = 84%  Analysis Date = 02/13/16 
 Pct Recovery = 84%  Analysis Date = 02/09/16 
 Pct Recovery = 84%  Analysis Date = 02/09/16 
 Pct Recovery = 84%  Analysis Date = 02/05/16 
 Pct Recovery = 84%  Analysis Date = 02/05/16 
 Pct Recovery = 84%  Analysis Date = 02/01/16 
 Pct Recovery = 84%  Analysis Date = 02/01/16 
 Pct Recovery = 84%  Analysis Date = 01/28/16 
 Pct Recovery = 84%  Analysis Date = 01/28/16 
 Pct Recovery = 84%  Analysis Date = 01/24/16 
 Pct Recovery = 84%  Analysis Date = 01/24/16 
 Pct Recovery = 84%  Analysis Date = 01/20/16 
 Pct Recovery = 84%  Analysis Date = 01/20/16 
 Pct Recovery = 84%  Analysis Date = 01/16/16 
 Pct Recovery = 84%  Analysis Date = 01/16/16 
 Pct Recovery = 84%  Analysis Date = 01/12/16 
 Pct Recovery = 84%  Analysis Date = 01/12/16 
 Pct Recovery = 84%  Analysis Date = 01/08/16 
 Pct Recovery = 84%  Analysis Date = 01/08/16 
 Pct Recovery = 84%  Analysis Date = 01/04/16 
 Pct Recovery = 84%  Analysis Date = 01/04/16 
 Pct Recovery = 84%  Analysis Date = 12/31/15 
 Pct Recovery = 84%  Analysis Date = 12/31/15 
 Pct Recovery = 84%  Analysis Date = 12/27/15 
 Pct Recovery = 85%  Analysis Date = 12/27/15 
 Pct Recovery = 85%  Analysis Date = 12/23/15 
 Pct Recovery = 85%  Analysis Date = 12/23/15 
 Pct Recovery = 85%  Analysis Date = 12/18/15 
 Pct Recovery = 85%  Analysis Date = 12/18/15 
 Pct Recovery = 85%  Analysis Date = 12/14/15 
 Pct Recovery = 85%  Analysis Date = 12/14/15 
 Pct Recovery = 85%  Analysis Date = 12/10/15 
 Pct Recovery = 85%  Analysis Date = 12/10/15 
 Pct Recovery = 85%  Analysis Date = 12/06/15 
 Pct Recovery = 85%  Analysis Date = 12/06/15 
 Pct Recovery = 85%  Analysis Date = 12/02/15 
 Pct Recovery = 85%  Analysis Date = 12/02/15 
 Pct Recovery = 85%  Analysis Date = 11/28/15 
 Pct Recovery = 85%  Analysis Date = 11/28/15 
 Pct Recovery = 85%  Analysis Date = 11/24/15 
 Pct Recovery = 85%  Analysis Date = 11/24/15 
 Pct Recovery = 85%  Analysis Date = 11/20/15 
 Pct Recovery = 85%  Analysis Date = 11/20/15 
 Pct Recovery = 85%  Analysis Date = 11/16/15 
 Pct Recovery = 85%  Analysis Date = 11/16/15 
 Pct Recovery = 85%  Analysis Date = 11/12/15 
 Pct Recovery = 84%  Analysis Date = 11/12/15 
 Pct Recovery = 84%  Analysis Date = 11/08/15 
 Pct Recovery = 84%  Analysis Date = 11/08/15 
 Pct Recovery = 84%  Analysis Date = 11/04/15 
 Pct Recovery = 84%  Analysis Date = 11/04/15 
 Pct Recovery = 84%  Analysis Date = 10/31/15 
 Pct Recovery = 84%  Analysis Date = 10/31/15 
 Pct Recovery = 84%  Analysis Date = 10/27/15 
 Pct Recovery = 84%  Analysis Date = 10/27/15 
 Pct Recovery = 84%  Analysis Date = 10/22/15 
 Pct Recovery = 84%  Analysis Date = 10/22/15 
 Pct Recovery = 84%  Analysis Date = 10/18/15 
 Pct Recovery = 84%  Analysis Date = 10/18/15 
 Pct Recovery = 84%  Analysis Date = 10/14/15 
 Pct Recovery = 84%  Analysis Date = 10/14/15 
 Pct Recovery = 84%  Analysis Date = 10/10/15 
 Pct Recovery = 84%  Analysis Date = 10/10/15 
 Pct Recovery = 84%  Analysis Date = 10/06/15 
 Pct Recovery = 84%  Analysis Date = 10/06/15 
 Pct Recovery = 84%  Analysis Date = 10/02/15 
 Pct Recovery = 84%  Analysis Date = 10/02/15 
 Pct Recovery = 84%  Analysis Date = 09/28/15 
 Pct Recovery = 84%  Analysis Date = 09/28/15 
 Pct Recovery = 84%  Analysis Date = 09/24/15 
 Pct Recovery = 84%  Analysis Date = 09/24/15 
 Pct Recovery = 84%  Analysis Date = 09/20/15 
 Pct Recovery = 84%  Analysis Date = 09/20/15 
 Pct Recovery = 84%  Analysis Date = 09/16/15 
 Pct Recovery = 84%  Analysis Date = 09/16/15 
 Pct Recovery = 84%  Analysis Date = 09/12/15 
 Pct Recovery = 84%  Analysis Date = 09/12/15 
 Pct Recovery = 84%  Analysis Date = 09/08/15 
 Pct Recovery = 84%  Analysis Date = 09/08/15 
 Pct Recovery = 84%  Analysis Date = 09/04/15 
 Pct Recovery = 84%  Analysis Date = 09/04/15 
 Pct Recovery = 84%  Analysis Date = 08/31/15 
 Pct Recovery = 84%  Analysis Date = 08/31/15 
 Pct Recovery = 84%  Analysis Date = 08/26/15 
 Pct Recovery = 84%  Analysis Date = 08/26/15 
 Pct Recovery = 84%  Analysis Date = 08/22/15 
 Pct Recovery = 84%  Analysis Date = 08/22/15 
 Pct Recovery = 84%  Analysis Date = 08/18/15 
 Pct Recovery = 84%  Analysis Date = 08/18/15 
 Pct Recovery = 84%  Analysis Date = 08/14/15 
 Pct Recovery = 84%  Analysis Date = 08/14/15 
 Pct Recovery = 84%  Analysis Date = 08/10/15 
 Pct Recovery = 85%  Analysis Date = 08/10/15 
 Pct Recovery = 85%  Analysis Date = 08/06/15 
 Pct Recovery = 85%  Analysis Date = 08/06/15 
 Pct Recovery = 85%  Analysis Date = 08/02/15 
 Pct Recovery = 85%  Analysis Date = 08/02/15 
 Pct Recovery = 85%  Analysis Date = 07/29/15 
 Pct Recovery = 85%  Analysis Date = 07/29/15 
 Pct Recovery = 85%  Analysis Date = 07/25/15 
 Pct Recovery = 85%  Analysis Date = 07/25/15 
 Pct Recovery = 85%  Analysis Date = 07/21/15 
 Pct Recovery = 86%  Analysis Date = 07/21/15 
 Pct Recovery = 86%  Analysis Date = 07/17/15 
 Pct Recovery = 86%  Analysis Date = 07/17/15 
 Pct Recovery = 86%  Analysis Date = 07/13/15 
 Pct Recovery = 86%  Analysis Date = 07/13/15 
 Pct Recovery = 86%  Analysis Date = 07/09/15 
 Pct Recovery = 86%  Analysis Date = 07/09/15 
 Pct Recovery = 86%  Analysis Date = 07/05/15 
 Pct Recovery = 86%  Analysis Date = 07/05/15 
 Pct Recovery = 86%  Analysis Date = 06/30/15 
 Pct Recovery = 87%  Analysis Date = 06/30/15 
 Pct Recovery = 87%  Analysis Date = 06/26/15 
 Pct Recovery = 87%  Analysis Date = 06/26/15 
 Pct Recovery = 87%  Analysis Date = 06/22/15 
 Pct Recovery = 87%  Analysis Date = 06/22/15 
 Pct Recovery = 87%  Analysis Date = 06/18/15 
 Pct Recovery = 87%  Analysis Date = 06/18/15 
 Pct Recovery = 87%  Analysis Date = 06/14/15 
 Pct Recovery = 87%  Analysis Date = 06/14/15 
 Pct Recovery = 87%  Analysis Date = 06/10/15 
 Pct Recovery = 88%  Analysis Date = 06/10/15 
 Pct Recovery = 88%  Analysis Date = 06/06/15 
 Pct Recovery = 88%  Analysis Date = 06/06/15 
 Pct Recovery = 88%  Analysis Date = 06/02/15 
 Pct Recovery = 88%  Analysis Date = 06/02/15 
 Pct Recovery = 88%  Analysis Date = 05/29/15 
 Pct Recovery = 88%  Analysis Date = 05/29/15 
 Pct Recovery = 88%  Analysis Date = 05/25/15 
 Pct Recovery = 88%  Analysis Date = 05/25/15 
 Pct Recovery = 88%  Analysis Date = 05/21/15 
 Pct Recovery = 89%  Analysis Date = 05/21/15 
 Pct Recovery = 89%  Analysis Date = 05/17/15 
 Pct Recovery = 89%  Analysis Date = 05/17/15 
 Pct Recovery = 89%  Analysis Date = 05/13/15 
 Pct Recovery = 89%  Analysis Date = 05/13/15 
 Pct Recovery = 89%  Analysis Date = 05/09/15 
 Pct Recovery = 89%  Analysis Date = 05/09/15 
 Pct Recovery = 89%  Analysis Date = 05/05/15 
 Pct Recovery = 89%  Analysis Date = 05/05/15 
 Pct Recovery = 89%  Analysis Date = 04/30/15 
 Pct Recovery = 90%  Analysis Date = 04/30/15 
 Pct Recovery = 90%  Analysis Date = 04/26/15 
 Pct Recovery = 90%  Analysis Date = 04/26/15 
 Pct Recovery = 90%  Analysis Date = 04/22/15 
 Pct Recovery = 90%  Analysis Date = 04/22/15 
 Pct Recovery = 90%  Analysis Date = 04/18/15 
 Pct Recovery = 90%  Analysis Date = 04/18/15 
 Pct Recovery = 90%  Analysis Date = 04/14/15 
 Pct Recovery = 91%  Analysis Date = 04/14/15 
 Pct Recovery = 91%  Analysis Date = 04/10/15 
 Pct Recovery = 91%  Analysis Date = 04/10/15 
 Pct Recovery = 91%  Analysis Date = 04/06/15 
 Pct Recovery = 91%  Analysis Date = 04/06/15 
 Pct Recovery = 91%  Analysis Date = 04/02/15 
 Pct Recovery = 92%  Analysis Date = 04/02/15 
 Pct Recovery = 92%  Analysis Date = 03/29/15 
 Pct Recovery = 92%  Analysis Date = 03/29/15 
 Pct Recovery = 92%  Analysis Date = 03/25/15 
 Pct Recovery = 92%  Analysis Date = 03/25/15 
 Pct Recovery = 92%  Analysis Date = 03/21/15 
 Pct Recovery = 92%  Analysis Date = 03/21/15 
 Pct Recovery = 92%  Analysis Date = 03/17/15 
 Pct Recovery = 93%  Analysis Date = 03/17/15 
 Pct Recovery = 93%  Analysis Date = 03/13/15 
 Pct Recovery = 93%  Analysis Date = 03/13/15 
 Pct Recovery = 93%  Analysis Date = 03/09/15 
 Pct Recovery = 93%  Analysis Date = 03/09/15 
 Pct Recovery = 93%  Analysis Date = 03/04/15 
 Pct Recovery = 93%  Analysis Date = 03/04/15 
 Pct Recovery = 93%  Analysis Date = 02/28/15 
 Pct Recovery = 94%  Analysis Date = 02/28/15 
 Pct Recovery = 94%  Analysis Date = 02/24/15 
 Pct Recovery = 94%  Analysis Date = 02/24/15 
 Pct Recovery = 94%  Analysis Date = 02/20/15 
 Pct Recovery = 94%  Analysis Date = 02/20/15 
 Pct Recovery = 94%  Analysis Date = 02/16/15 
 Pct Recovery = 95%  Analysis Date = 02/16/15 
 Pct Recovery = 95%  Analysis Date = 02/12/15 
 Pct Recovery = 95%  Analysis Date = 02/12/15 
 Pct Recovery = 95%  Analysis Date = 02/08/15 
 Pct Recovery = 95%  Analysis Date = 02/08/15 
 Pct Recovery = 95%  Analysis Date = 02/04/15 
 Pct Recovery = 95%  Analysis Date = 02/04/15 
 Pct Recovery = 95%  Analysis Date = 01/31/15 
 Pct Recovery = 96%  Analysis Date = 01/31/15 
 Pct Recovery = 96%  Analysis Date = 01/27/15 
 Pct Recovery = 96%  Analysis Date = 01/27/15 
 Pct Recovery = 96%  Analysis Date = 01/23/15 
 Pct Recovery = 96%  Analysis Date = 01/23/15 
 Pct Recovery = 96%  Analysis Date = 01/19/15 
 Pct Recovery = 96%  Analysis Date = 01/19/15 
 Pct Recovery = 96%  Analysis Date = 01/15/15 
 Pct Recovery = 97%  Analysis Date = 01/15/15 
 Pct Recovery = 97%  Analysis Date = 01/11/15 
 Pct Recovery = 97%  Analysis Date = 01/11/15 
 Pct Recovery = 97%  Analysis Date = 01/06/15 
 Pct Recovery = 97%  Analysis Date = 01/06/15 
 Pct Recovery = 97%  Analysis Date = 01/02/15 
 Pct Recovery = 97%  Analysis Date = 01/02/15 
 Pct Recovery = 97%  Analysis Date = 12/29/14 
 Pct Recovery = 98%  Analysis Date = 12/29/14 
 Pct Recovery = 98%  Analysis Date = 12/25/14 
 Pct Recovery = 98%  Analysis Date = 12/25/14 
 Pct Recovery = 98%  Analysis Date = 12/21/14 
 Pct Recovery = 98%  Analysis Date = 12/21/14 
 Pct Recovery = 98%  Analysis Date = 12/17/14 
 Pct Recovery = 99%  Analysis Date = 12/17/14 
 Pct Recovery = 99%  Analysis Date = 12/13/14 
 Pct Recovery = 99%  Analysis Date = 12/13/14 
 Pct Recovery = 99%  Analysis Date = 12/09/14 
 Pct Recovery = 99%  Analysis Date = 12/09/14 
 Pct Recovery = 99%  Analysis Date = 12/05/14 
 Pct Recovery = 99%  Analysis Date = 12/05/14 
 Pct Recovery = 99%  Analysis Date = 12/01/14 
 Pct Recovery = 100%  Analysis Date = 12/01/14 
 Pct Recovery = 100%  Analysis Date = 11/27/14 
 Pct Recovery = 100%  Analysis Date = 11/27/14 
 Pct Recovery = 100%  Analysis Date = 11/23/14 
 Pct Recovery = 100%  Analysis Date = 11/23/14 
 Pct Recovery = 100%  Analysis Date = 11/19/14 
 Pct Recovery = 100%  Analysis Date = 11/19/14 
 Pct Recovery = 100%  Analysis Date = 11/15/14 
 Pct Recovery = 101%  Analysis Date = 11/15/14 
 Pct Recovery = 101%  Analysis Date = 11/11/14 
 Pct Recovery = 101%  Analysis Date = 11/11/14 
 Pct Recovery = 101%  Analysis Date = 11/06/14 
 Pct Recovery = 101%  Analysis Date = 11/06/14 
 Pct Recovery = 101%  Analysis Date = 11/02/14 
 Pct Recovery = 102%  Analysis Date = 11/02/14 
 Pct Recovery = 102%  Analysis Date = 10/29/14 
 Pct Recovery = 102%  Analysis Date = 10/29/14 
 Pct Recovery = 102%  Analysis Date = 10/25/14 
 Pct Recovery = 102%  Analysis Date = 10/25/14 
 Pct Recovery = 102%  Analysis Date = 10/21/14 
 Pct Recovery = 102%  Analysis Date = 10/21/14 
 Pct Recovery = 102%  Analysis Date = 10/17/14 
 Pct Recovery = 103%  Analysis Date = 10/17/14 
 Pct Recovery = 103%  Analysis Date = 10/13/14 
 Pct Recovery = 103%  Analysis Date = 10/13/14 
 Pct Recovery = 103%  Analysis Date = 10/09/14 
 Pct Recovery = 103%  Analysis Date = 10/09/14 
 Pct Recovery = 103%  Analysis Date = 10/05/14 
 Pct Recovery = 103%  Analysis Date = 10/05/14 
 Pct Recovery = 103%  Analysis Date = 10/01/14 
 Pct Recovery = 103%  Analysis Date = 10/01/14 
 Pct Recovery = 103%  Analysis Date = 09/27/14 
 Pct Recovery = 104%  Analysis Date = 09/27/14 
 Pct Recovery = 104%  Analysis Date = 09/23/14 
 Pct Recovery = 104%  Analysis Date = 09/23/14 
 Pct Recovery = 104%  Analysis Date = 09/19/14 
 Pct Recovery = 104%  Analysis Date = 09/19/14 
 Pct Recovery = 104%  Analysis Date = 09/15/14 
 Pct Recovery = 104%  Analysis Date = 09/15/14 
 Pct Recovery = 104%  Analysis Date = 09/10/14 
 Pct Recovery = 104%  Analysis Date = 09/10/14 
 Pct Recovery = 104%  Analysis Date = 09/06/14 
 Pct Recovery = 104%  Analysis Date = 09/06/14 
 Pct Recovery = 104%  Analysis Date = 09/02/14 
 Pct Recovery = 105%  Analysis Date = 09/02/14 
 Pct Recovery = 105%  Analysis Date = 08/29/14 
 Pct Recovery = 105%  Analysis Date = 08/29/14 
 Pct Recovery = 105%  Analysis Date = 08/25/14 
 Pct Recovery = 105%  Analysis Date = 08/25/14 
 Pct Recovery = 105%  Analysis Date = 08/21/14 
 Pct Recovery = 105%  Analysis Date = 08/21/14 
 Pct Recovery = 105%  Analysis Date = 08/17/14 
 Pct Recovery = 105%  Analysis Date = 08/17/14 
 Pct Recovery = 105%  Analysis Date = 08/13/14 
 Pct Recovery = 106%  Analysis Date = 08/13/14 
 Pct Recovery = 106%  Analysis Date = 08/09/14 
 Pct Recovery = 106%  Analysis Date = 08/09/14 
 Pct Recovery = 106%  Analysis Date = 08/05/14 
 Pct Recovery = 106%  Analysis Date = 08/05/14 
 Pct Recovery = 106%  Analysis Date = 08/01/14 
 Pct Recovery = 106%  Analysis Date = 08/01/14 
 Pct Recovery = 106%  Analysis Date = 07/28/14 
 Pct Recovery = 106%  Analysis Date = 07/28/14 
 Pct Recovery = 106%  Analysis Date = 07/24/14 
 Pct Recovery = 107%  Analysis Date = 07/24/14 
 Pct Recovery = 107%  Analysis Date = 07/20/14 
 Pct Recovery = 107%  Analysis Date = 07/20/14 
 Pct Recovery = 107%  Analysis Date = 07/15/14 
 Pct Recovery = 107%  Analysis Date = 07/15/14 
 Pct Recovery = 107%  Analysis Date = 07/11/14 
 Pct Recovery = 107%  Analysis Date = 07/11/14 
 Pct Recovery = 107%  Analysis Date = 07/07/14 
 Pct Recovery = 107%  Analysis Date = 07/07/14 
 Pct Recovery = 107%  Analysis Date = 07/03/14 
 Pct Recovery = 108%  Analysis Date = 07/03/14 
 Pct Recovery = 108%  Analysis Date = 06/29/14 
 Pct Recovery = 108%  Analysis Date = 06/29/14 
 Pct Recovery = 108%  Analysis Date = 06/25/14 
 Pct Recovery = 108%  Analysis Date = 06/25/14 
 Pct Recovery = 108%  Analysis Date = 06/21/14 
 Pct Recovery = 108%  Analysis Date = 06/21/14 
 Pct Recovery = 108%  Analysis Date = 06/17/14 
 Pct Recovery = 108%  Analysis Date = 06/17/14 
 Pct Recovery = 108%  Analysis Date = 06/13/14 
 Pct Recovery = 108%  Analysis Date = 06/13/14 
 Pct Recovery = 108%  Analysis Date = 06/09/14 
 Pct Recovery = 109%  Analysis Date = 06/09/14 
 Pct Recovery = 109%  Analysis Date = 06/05/14 
 Pct Recovery = 109%  Analysis Date = 06/05/14 
 Pct Recovery = 109%  Analysis Date = 06/01/14 
 Pct Recovery = 109%  Analysis Date = 06/01/14 
 Pct Recovery = 109%  Analysis Date = 05/28/14 
 Pct Recovery = 109%  Analysis Date = 05/28/14 
 Pct Recovery = 109%  Analysis Date = 05/24/14 
 Pct Recovery = 109%  Analysis Date = 05/24/14 
 Pct Recovery = 109%  Analysis Date = 05/20/14 
 Pct Recovery = 109%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
DIETHYLAMINE, N-NITROSO-

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 34 91% 17% 92% 15%
Total 34 91% 17% 92% 15%

Sample Statistics
DIETHYLAMINE, N-NITROSO-

Characteristic N % % Basis
Plotted 34 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 34 .  
False Negatives 0 0% 0 out of 34
Not Spiked 21 .  
False Positives 0 0% 0 out of 21

BQS OBSP Determination:
DIMETHOXYMETHANE
METHOD: 4437 , TESTIDCODE: 81578GM016
Open Data Set

 Analysis Date = 07/29/16 
 SpikeMix = Supelco LC20145V: 40 µl & NSI 041516: 40 µl & NSI 041416HVOC: 40 µl 
 Pct Recovery = 108%  Analysis Date = 07/06/16 
 SpikeMix = Accu 216041354: 40 µl & NSI 041516: 40 µl & NSI 041416HVOC: 40 µl 
 Pct Recovery = 92%  Analysis Date = 08/11/16 
 SpikeMix = Phenova B20160303: 25 µl & Supelco LC20145V: 25 µl & NSI 041416HVOC: 25 µl 
 Pct Recovery = 106%  Analysis Date = 05/26/16 
 SpikeMix = Supelco LC20145V: 25 µl & NSI 041516: 25 µl & NSI 041416HVOC: 25 µl 
 Pct Recovery = 129%  Analysis Date = 03/19/15 
 SpikeMix = Supelco LC06437: 20 µl & NSI 031814: 20 µl 
 Pct Recovery = 115%  Analysis Date = 08/20/14 
 SpikeMix = Supelco LC06437: 20 µl & Abs 032014: 20 µl 
 Pct Recovery = 109%  Analysis Date = 06/07/14 
 SpikeMix = ChemService 2615700: 20 µl & Supelco LC06437: 20 µl 
 Pct Recovery = 114%  Analysis Date = 10/09/15 
 SpikeMix = Supelco LC13544: 25 µl & NSI 050515HVOC: 25 µl 
 Pct Recovery = 162%  Analysis Date = 06/25/15 
 SpikeMix = ChemService 3818700: 25 µl & NSI 050515HVOC: 25 µl 
 Pct Recovery = 152%  Analysis Date = 07/23/14 
 SpikeMix = Accu 214031128: 20 µl & Abs 032014: 20 µl 
 Pct Recovery = 91%  Analysis Date = 07/11/14 
 SpikeMix = ChemService 2615700: 20 µl & Accu 214031128: 20 µl 
 Pct Recovery = 90%  Analysis Date = 05/07/14 
 SpikeMix = NSI 031814: 20 µl & Accu 214031128: 20 µl 
 Pct Recovery = 84%  Analysis Date = 08/12/16 
 SpikeMix = Accu 216041354: 15 µl & Abs 060916HVOC: 15 µl 
 Pct Recovery = 102%  Analysis Date = 07/27/16 
 SpikeMix = ChemService 5082800: 15 µl & Supelco LC20145V: 15 µl & Accu 216041225: 15 µl 
 Pct Recovery = 108%  Analysis Date = 07/06/16 
 SpikeMix = Phenova B20160303: 15 µl & Accu 216041354: 15 µl & NSI 041416HVOC: 15 µl 
 Pct Recovery = 92%  Analysis Date = 06/23/16 
 SpikeMix = . 
 Pct Recovery = 104%  Analysis Date = 05/26/16 
 SpikeMix = Accu 216041354: 15 µl & NSI 041516: 15 µl & Accu 216041225: 15 µl 
 Pct Recovery = 104%  Analysis Date = 11/25/15 
 SpikeMix = Accu 215041338: 15 µl & Abs 040315: 15 µl 
 Pct Recovery = 114%  Analysis Date = 09/05/15 
 SpikeMix = Accu 215041338: 15 µl & NSI 050515HVOC: 15 µl 
 Pct Recovery = 140%  Analysis Date = 07/30/15 
 SpikeMix = Supelco LC13544: 15 µl & NSI 050515HVOC: 15 µl 
 Pct Recovery = 156%  Analysis Date = 06/16/15 
 SpikeMix = ChemService 3818700: 15 µl & NSI 050515HVOC: 15 µl 
 Pct Recovery = 146%  Analysis Date = 11/22/14 
 SpikeMix = ChemService 2615700: 10 µl & Supelco LC06437: 10 µl 
 Pct Recovery = 105%  Analysis Date = 06/17/14 
 SpikeMix = Supelco LC06437: 10 µl & Abs 032014: 10 µl 
 Pct Recovery = 107%  Analysis Date = 12/13/14 
 SpikeMix = Accu 214031128: 10 µl & NSI 031814: 10 µl 
 Pct Recovery = 83%  Analysis Date = 09/11/14 
 SpikeMix = Accu 214031128: 10 µl & Abs 032014: 10 µl 
 Pct Recovery = 86%  Analysis Date = 05/20/14 
 SpikeMix = ChemService 2615700: 10 µl & Accu 214031128: 10 µl 
 Pct Recovery = 87%  Analysis Date = 04/09/16 
 SpikeMix = Abs 040315: 10 µl & ChemService 3818700: 10 µl 
 Pct Recovery = 114%  Analysis Date = 03/22/16 
 SpikeMix = Supelco LC13544: 10 µl & NSI 050515HVOC: 10 µl 
 Pct Recovery = 182%  Analysis Date = 01/05/16 
 SpikeMix = Accu 215041338: 10 µl & Abs 040315: 10 µl 
 Pct Recovery = 118%  Analysis Date = 10/23/15 
 SpikeMix = Abs 040315: 10 µl & ChemService 3818700: 10 µl 
 Pct Recovery = 133%  Analysis Date = 05/05/15 
 SpikeMix = Supelco LC13544: 10 µl & Abs 040315: 10 µl 
 Pct Recovery = 105%  Analysis Date = 08/11/16 
 Pct Recovery = 102%  Analysis Date = 08/07/16 
 Pct Recovery = 103%  Analysis Date = 08/07/16 
 Pct Recovery = 103%  Analysis Date = 08/03/16 
 Pct Recovery = 103%  Analysis Date = 08/03/16 
 Pct Recovery = 103%  Analysis Date = 07/30/16 
 Pct Recovery = 104%  Analysis Date = 07/30/16 
 Pct Recovery = 104%  Analysis Date = 07/26/16 
 Pct Recovery = 105%  Analysis Date = 07/26/16 
 Pct Recovery = 105%  Analysis Date = 07/22/16 
 Pct Recovery = 105%  Analysis Date = 07/22/16 
 Pct Recovery = 105%  Analysis Date = 07/18/16 
 Pct Recovery = 106%  Analysis Date = 07/18/16 
 Pct Recovery = 106%  Analysis Date = 07/14/16 
 Pct Recovery = 107%  Analysis Date = 07/14/16 
 Pct Recovery = 107%  Analysis Date = 07/09/16 
 Pct Recovery = 107%  Analysis Date = 07/09/16 
 Pct Recovery = 107%  Analysis Date = 07/05/16 
 Pct Recovery = 108%  Analysis Date = 07/05/16 
 Pct Recovery = 108%  Analysis Date = 07/01/16 
 Pct Recovery = 108%  Analysis Date = 07/01/16 
 Pct Recovery = 108%  Analysis Date = 06/27/16 
 Pct Recovery = 109%  Analysis Date = 06/27/16 
 Pct Recovery = 109%  Analysis Date = 06/23/16 
 Pct Recovery = 110%  Analysis Date = 06/23/16 
 Pct Recovery = 110%  Analysis Date = 06/19/16 
 Pct Recovery = 110%  Analysis Date = 06/19/16 
 Pct Recovery = 110%  Analysis Date = 06/15/16 
 Pct Recovery = 111%  Analysis Date = 06/15/16 
 Pct Recovery = 111%  Analysis Date = 06/10/16 
 Pct Recovery = 111%  Analysis Date = 06/10/16 
 Pct Recovery = 111%  Analysis Date = 06/06/16 
 Pct Recovery = 112%  Analysis Date = 06/06/16 
 Pct Recovery = 112%  Analysis Date = 06/02/16 
 Pct Recovery = 113%  Analysis Date = 06/02/16 
 Pct Recovery = 113%  Analysis Date = 05/29/16 
 Pct Recovery = 113%  Analysis Date = 05/29/16 
 Pct Recovery = 113%  Analysis Date = 05/25/16 
 Pct Recovery = 114%  Analysis Date = 05/25/16 
 Pct Recovery = 114%  Analysis Date = 05/21/16 
 Pct Recovery = 114%  Analysis Date = 05/21/16 
 Pct Recovery = 114%  Analysis Date = 05/17/16 
 Pct Recovery = 115%  Analysis Date = 05/17/16 
 Pct Recovery = 115%  Analysis Date = 05/12/16 
 Pct Recovery = 115%  Analysis Date = 05/12/16 
 Pct Recovery = 115%  Analysis Date = 05/08/16 
 Pct Recovery = 116%  Analysis Date = 05/08/16 
 Pct Recovery = 116%  Analysis Date = 05/04/16 
 Pct Recovery = 116%  Analysis Date = 05/04/16 
 Pct Recovery = 116%  Analysis Date = 04/30/16 
 Pct Recovery = 117%  Analysis Date = 04/30/16 
 Pct Recovery = 117%  Analysis Date = 04/26/16 
 Pct Recovery = 118%  Analysis Date = 04/26/16 
 Pct Recovery = 118%  Analysis Date = 04/22/16 
 Pct Recovery = 118%  Analysis Date = 04/22/16 
 Pct Recovery = 118%  Analysis Date = 04/18/16 
 Pct Recovery = 119%  Analysis Date = 04/18/16 
 Pct Recovery = 119%  Analysis Date = 04/13/16 
 Pct Recovery = 119%  Analysis Date = 04/13/16 
 Pct Recovery = 119%  Analysis Date = 04/09/16 
 Pct Recovery = 120%  Analysis Date = 04/09/16 
 Pct Recovery = 120%  Analysis Date = 04/05/16 
 Pct Recovery = 120%  Analysis Date = 04/05/16 
 Pct Recovery = 120%  Analysis Date = 04/01/16 
 Pct Recovery = 121%  Analysis Date = 04/01/16 
 Pct Recovery = 121%  Analysis Date = 03/28/16 
 Pct Recovery = 122%  Analysis Date = 03/28/16 
 Pct Recovery = 122%  Analysis Date = 03/24/16 
 Pct Recovery = 122%  Analysis Date = 03/24/16 
 Pct Recovery = 122%  Analysis Date = 03/20/16 
 Pct Recovery = 123%  Analysis Date = 03/20/16 
 Pct Recovery = 123%  Analysis Date = 03/15/16 
 Pct Recovery = 123%  Analysis Date = 03/15/16 
 Pct Recovery = 123%  Analysis Date = 03/11/16 
 Pct Recovery = 124%  Analysis Date = 03/11/16 
 Pct Recovery = 124%  Analysis Date = 03/07/16 
 Pct Recovery = 125%  Analysis Date = 03/07/16 
 Pct Recovery = 125%  Analysis Date = 03/03/16 
 Pct Recovery = 125%  Analysis Date = 03/03/16 
 Pct Recovery = 125%  Analysis Date = 02/28/16 
 Pct Recovery = 126%  Analysis Date = 02/28/16 
 Pct Recovery = 126%  Analysis Date = 02/24/16 
 Pct Recovery = 126%  Analysis Date = 02/24/16 
 Pct Recovery = 126%  Analysis Date = 02/20/16 
 Pct Recovery = 127%  Analysis Date = 02/20/16 
 Pct Recovery = 127%  Analysis Date = 02/15/16 
 Pct Recovery = 128%  Analysis Date = 02/15/16 
 Pct Recovery = 128%  Analysis Date = 02/11/16 
 Pct Recovery = 128%  Analysis Date = 02/11/16 
 Pct Recovery = 128%  Analysis Date = 02/07/16 
 Pct Recovery = 129%  Analysis Date = 02/07/16 
 Pct Recovery = 129%  Analysis Date = 02/03/16 
 Pct Recovery = 129%  Analysis Date = 02/03/16 
 Pct Recovery = 129%  Analysis Date = 01/30/16 
 Pct Recovery = 130%  Analysis Date = 01/30/16 
 Pct Recovery = 130%  Analysis Date = 01/26/16 
 Pct Recovery = 131%  Analysis Date = 01/26/16 
 Pct Recovery = 131%  Analysis Date = 01/22/16 
 Pct Recovery = 131%  Analysis Date = 01/22/16 
 Pct Recovery = 131%  Analysis Date = 01/17/16 
 Pct Recovery = 132%  Analysis Date = 01/17/16 
 Pct Recovery = 132%  Analysis Date = 01/13/16 
 Pct Recovery = 133%  Analysis Date = 01/13/16 
 Pct Recovery = 133%  Analysis Date = 01/09/16 
 Pct Recovery = 133%  Analysis Date = 01/09/16 
 Pct Recovery = 133%  Analysis Date = 01/05/16 
 Pct Recovery = 134%  Analysis Date = 01/05/16 
 Pct Recovery = 134%  Analysis Date = 01/01/16 
 Pct Recovery = 134%  Analysis Date = 01/01/16 
 Pct Recovery = 134%  Analysis Date = 12/28/15 
 Pct Recovery = 134%  Analysis Date = 12/28/15 
 Pct Recovery = 134%  Analysis Date = 12/24/15 
 Pct Recovery = 134%  Analysis Date = 12/24/15 
 Pct Recovery = 134%  Analysis Date = 12/20/15 
 Pct Recovery = 135%  Analysis Date = 12/20/15 
 Pct Recovery = 135%  Analysis Date = 12/15/15 
 Pct Recovery = 135%  Analysis Date = 12/15/15 
 Pct Recovery = 135%  Analysis Date = 12/11/15 
 Pct Recovery = 135%  Analysis Date = 12/11/15 
 Pct Recovery = 135%  Analysis Date = 12/07/15 
 Pct Recovery = 135%  Analysis Date = 12/07/15 
 Pct Recovery = 135%  Analysis Date = 12/03/15 
 Pct Recovery = 136%  Analysis Date = 12/03/15 
 Pct Recovery = 136%  Analysis Date = 11/29/15 
 Pct Recovery = 136%  Analysis Date = 11/29/15 
 Pct Recovery = 136%  Analysis Date = 11/25/15 
 Pct Recovery = 136%  Analysis Date = 11/25/15 
 Pct Recovery = 136%  Analysis Date = 11/21/15 
 Pct Recovery = 136%  Analysis Date = 11/21/15 
 Pct Recovery = 136%  Analysis Date = 11/16/15 
 Pct Recovery = 136%  Analysis Date = 11/16/15 
 Pct Recovery = 136%  Analysis Date = 11/12/15 
 Pct Recovery = 137%  Analysis Date = 11/12/15 
 Pct Recovery = 137%  Analysis Date = 11/08/15 
 Pct Recovery = 137%  Analysis Date = 11/08/15 
 Pct Recovery = 137%  Analysis Date = 11/04/15 
 Pct Recovery = 137%  Analysis Date = 11/04/15 
 Pct Recovery = 137%  Analysis Date = 10/31/15 
 Pct Recovery = 137%  Analysis Date = 10/31/15 
 Pct Recovery = 137%  Analysis Date = 10/27/15 
 Pct Recovery = 138%  Analysis Date = 10/27/15 
 Pct Recovery = 138%  Analysis Date = 10/23/15 
 Pct Recovery = 138%  Analysis Date = 10/23/15 
 Pct Recovery = 138%  Analysis Date = 10/18/15 
 Pct Recovery = 138%  Analysis Date = 10/18/15 
 Pct Recovery = 138%  Analysis Date = 10/14/15 
 Pct Recovery = 138%  Analysis Date = 10/14/15 
 Pct Recovery = 138%  Analysis Date = 10/10/15 
 Pct Recovery = 137%  Analysis Date = 10/10/15 
 Pct Recovery = 137%  Analysis Date = 10/06/15 
 Pct Recovery = 137%  Analysis Date = 10/06/15 
 Pct Recovery = 137%  Analysis Date = 10/02/15 
 Pct Recovery = 137%  Analysis Date = 10/02/15 
 Pct Recovery = 137%  Analysis Date = 09/28/15 
 Pct Recovery = 137%  Analysis Date = 09/28/15 
 Pct Recovery = 137%  Analysis Date = 09/24/15 
 Pct Recovery = 137%  Analysis Date = 09/24/15 
 Pct Recovery = 137%  Analysis Date = 09/19/15 
 Pct Recovery = 137%  Analysis Date = 09/19/15 
 Pct Recovery = 137%  Analysis Date = 09/15/15 
 Pct Recovery = 137%  Analysis Date = 09/15/15 
 Pct Recovery = 137%  Analysis Date = 09/11/15 
 Pct Recovery = 137%  Analysis Date = 09/11/15 
 Pct Recovery = 137%  Analysis Date = 09/07/15 
 Pct Recovery = 137%  Analysis Date = 09/07/15 
 Pct Recovery = 137%  Analysis Date = 09/03/15 
 Pct Recovery = 137%  Analysis Date = 09/03/15 
 Pct Recovery = 137%  Analysis Date = 08/30/15 
 Pct Recovery = 136%  Analysis Date = 08/30/15 
 Pct Recovery = 136%  Analysis Date = 08/26/15 
 Pct Recovery = 136%  Analysis Date = 08/26/15 
 Pct Recovery = 136%  Analysis Date = 08/21/15 
 Pct Recovery = 135%  Analysis Date = 08/21/15 
 Pct Recovery = 135%  Analysis Date = 08/17/15 
 Pct Recovery = 135%  Analysis Date = 08/17/15 
 Pct Recovery = 135%  Analysis Date = 08/13/15 
 Pct Recovery = 135%  Analysis Date = 08/13/15 
 Pct Recovery = 135%  Analysis Date = 08/09/15 
 Pct Recovery = 134%  Analysis Date = 08/09/15 
 Pct Recovery = 134%  Analysis Date = 08/05/15 
 Pct Recovery = 134%  Analysis Date = 08/05/15 
 Pct Recovery = 134%  Analysis Date = 08/01/15 
 Pct Recovery = 133%  Analysis Date = 08/01/15 
 Pct Recovery = 133%  Analysis Date = 07/28/15 
 Pct Recovery = 133%  Analysis Date = 07/28/15 
 Pct Recovery = 133%  Analysis Date = 07/23/15 
 Pct Recovery = 132%  Analysis Date = 07/23/15 
 Pct Recovery = 132%  Analysis Date = 07/19/15 
 Pct Recovery = 132%  Analysis Date = 07/19/15 
 Pct Recovery = 132%  Analysis Date = 07/15/15 
 Pct Recovery = 132%  Analysis Date = 07/15/15 
 Pct Recovery = 132%  Analysis Date = 07/11/15 
 Pct Recovery = 131%  Analysis Date = 07/11/15 
 Pct Recovery = 131%  Analysis Date = 07/07/15 
 Pct Recovery = 131%  Analysis Date = 07/07/15 
 Pct Recovery = 131%  Analysis Date = 07/03/15 
 Pct Recovery = 130%  Analysis Date = 07/03/15 
 Pct Recovery = 130%  Analysis Date = 06/29/15 
 Pct Recovery = 130%  Analysis Date = 06/29/15 
 Pct Recovery = 130%  Analysis Date = 06/24/15 
 Pct Recovery = 130%  Analysis Date = 06/24/15 
 Pct Recovery = 130%  Analysis Date = 06/20/15 
 Pct Recovery = 129%  Analysis Date = 06/20/15 
 Pct Recovery = 129%  Analysis Date = 06/16/15 
 Pct Recovery = 129%  Analysis Date = 06/16/15 
 Pct Recovery = 129%  Analysis Date = 06/12/15 
 Pct Recovery = 128%  Analysis Date = 06/12/15 
 Pct Recovery = 128%  Analysis Date = 06/08/15 
 Pct Recovery = 128%  Analysis Date = 06/08/15 
 Pct Recovery = 128%  Analysis Date = 06/04/15 
 Pct Recovery = 127%  Analysis Date = 06/04/15 
 Pct Recovery = 127%  Analysis Date = 05/31/15 
 Pct Recovery = 127%  Analysis Date = 05/31/15 
 Pct Recovery = 127%  Analysis Date = 05/27/15 
 Pct Recovery = 127%  Analysis Date = 05/27/15 
 Pct Recovery = 127%  Analysis Date = 05/22/15 
 Pct Recovery = 126%  Analysis Date = 05/22/15 
 Pct Recovery = 126%  Analysis Date = 05/18/15 
 Pct Recovery = 126%  Analysis Date = 05/18/15 
 Pct Recovery = 126%  Analysis Date = 05/14/15 
 Pct Recovery = 125%  Analysis Date = 05/14/15 
 Pct Recovery = 125%  Analysis Date = 05/10/15 
 Pct Recovery = 125%  Analysis Date = 05/10/15 
 Pct Recovery = 125%  Analysis Date = 05/06/15 
 Pct Recovery = 124%  Analysis Date = 05/06/15 
 Pct Recovery = 124%  Analysis Date = 05/02/15 
 Pct Recovery = 124%  Analysis Date = 05/02/15 
 Pct Recovery = 124%  Analysis Date = 04/28/15 
 Pct Recovery = 123%  Analysis Date = 04/28/15 
 Pct Recovery = 123%  Analysis Date = 04/23/15 
 Pct Recovery = 123%  Analysis Date = 04/23/15 
 Pct Recovery = 123%  Analysis Date = 04/19/15 
 Pct Recovery = 122%  Analysis Date = 04/19/15 
 Pct Recovery = 122%  Analysis Date = 04/15/15 
 Pct Recovery = 122%  Analysis Date = 04/15/15 
 Pct Recovery = 122%  Analysis Date = 04/11/15 
 Pct Recovery = 122%  Analysis Date = 04/11/15 
 Pct Recovery = 122%  Analysis Date = 04/07/15 
 Pct Recovery = 121%  Analysis Date = 04/07/15 
 Pct Recovery = 121%  Analysis Date = 04/03/15 
 Pct Recovery = 121%  Analysis Date = 04/03/15 
 Pct Recovery = 121%  Analysis Date = 03/30/15 
 Pct Recovery = 120%  Analysis Date = 03/30/15 
 Pct Recovery = 120%  Analysis Date = 03/25/15 
 Pct Recovery = 120%  Analysis Date = 03/25/15 
 Pct Recovery = 120%  Analysis Date = 03/21/15 
 Pct Recovery = 119%  Analysis Date = 03/21/15 
 Pct Recovery = 119%  Analysis Date = 03/17/15 
 Pct Recovery = 119%  Analysis Date = 03/17/15 
 Pct Recovery = 119%  Analysis Date = 03/13/15 
 Pct Recovery = 118%  Analysis Date = 03/13/15 
 Pct Recovery = 118%  Analysis Date = 03/09/15 
 Pct Recovery = 118%  Analysis Date = 03/09/15 
 Pct Recovery = 118%  Analysis Date = 03/05/15 
 Pct Recovery = 117%  Analysis Date = 03/05/15 
 Pct Recovery = 117%  Analysis Date = 03/01/15 
 Pct Recovery = 117%  Analysis Date = 03/01/15 
 Pct Recovery = 117%  Analysis Date = 02/24/15 
 Pct Recovery = 116%  Analysis Date = 02/24/15 
 Pct Recovery = 116%  Analysis Date = 02/20/15 
 Pct Recovery = 116%  Analysis Date = 02/20/15 
 Pct Recovery = 116%  Analysis Date = 02/16/15 
 Pct Recovery = 116%  Analysis Date = 02/16/15 
 Pct Recovery = 116%  Analysis Date = 02/12/15 
 Pct Recovery = 115%  Analysis Date = 02/12/15 
 Pct Recovery = 115%  Analysis Date = 02/08/15 
 Pct Recovery = 115%  Analysis Date = 02/08/15 
 Pct Recovery = 115%  Analysis Date = 02/04/15 
 Pct Recovery = 114%  Analysis Date = 02/04/15 
 Pct Recovery = 114%  Analysis Date = 01/31/15 
 Pct Recovery = 114%  Analysis Date = 01/31/15 
 Pct Recovery = 114%  Analysis Date = 01/26/15 
 Pct Recovery = 113%  Analysis Date = 01/26/15 
 Pct Recovery = 113%  Analysis Date = 01/22/15 
 Pct Recovery = 113%  Analysis Date = 01/22/15 
 Pct Recovery = 113%  Analysis Date = 01/18/15 
 Pct Recovery = 112%  Analysis Date = 01/18/15 
 Pct Recovery = 112%  Analysis Date = 01/14/15 
 Pct Recovery = 112%  Analysis Date = 01/14/15 
 Pct Recovery = 112%  Analysis Date = 01/10/15 
 Pct Recovery = 111%  Analysis Date = 01/10/15 
 Pct Recovery = 111%  Analysis Date = 01/06/15 
 Pct Recovery = 111%  Analysis Date = 01/06/15 
 Pct Recovery = 111%  Analysis Date = 01/02/15 
 Pct Recovery = 110%  Analysis Date = 01/02/15 
 Pct Recovery = 110%  Analysis Date = 12/28/14 
 Pct Recovery = 110%  Analysis Date = 12/28/14 
 Pct Recovery = 110%  Analysis Date = 12/24/14 
 Pct Recovery = 110%  Analysis Date = 12/24/14 
 Pct Recovery = 110%  Analysis Date = 12/20/14 
 Pct Recovery = 109%  Analysis Date = 12/20/14 
 Pct Recovery = 109%  Analysis Date = 12/16/14 
 Pct Recovery = 109%  Analysis Date = 12/16/14 
 Pct Recovery = 109%  Analysis Date = 12/12/14 
 Pct Recovery = 108%  Analysis Date = 12/12/14 
 Pct Recovery = 108%  Analysis Date = 12/08/14 
 Pct Recovery = 108%  Analysis Date = 12/08/14 
 Pct Recovery = 108%  Analysis Date = 12/04/14 
 Pct Recovery = 107%  Analysis Date = 12/04/14 
 Pct Recovery = 107%  Analysis Date = 11/29/14 
 Pct Recovery = 107%  Analysis Date = 11/29/14 
 Pct Recovery = 107%  Analysis Date = 11/25/14 
 Pct Recovery = 107%  Analysis Date = 11/25/14 
 Pct Recovery = 107%  Analysis Date = 11/21/14 
 Pct Recovery = 106%  Analysis Date = 11/21/14 
 Pct Recovery = 106%  Analysis Date = 11/17/14 
 Pct Recovery = 106%  Analysis Date = 11/17/14 
 Pct Recovery = 106%  Analysis Date = 11/13/14 
 Pct Recovery = 106%  Analysis Date = 11/13/14 
 Pct Recovery = 106%  Analysis Date = 11/09/14 
 Pct Recovery = 105%  Analysis Date = 11/09/14 
 Pct Recovery = 105%  Analysis Date = 11/05/14 
 Pct Recovery = 105%  Analysis Date = 11/05/14 
 Pct Recovery = 105%  Analysis Date = 11/01/14 
 Pct Recovery = 105%  Analysis Date = 11/01/14 
 Pct Recovery = 105%  Analysis Date = 10/27/14 
 Pct Recovery = 104%  Analysis Date = 10/27/14 
 Pct Recovery = 104%  Analysis Date = 10/23/14 
 Pct Recovery = 104%  Analysis Date = 10/23/14 
 Pct Recovery = 104%  Analysis Date = 10/19/14 
 Pct Recovery = 103%  Analysis Date = 10/19/14 
 Pct Recovery = 103%  Analysis Date = 10/15/14 
 Pct Recovery = 103%  Analysis Date = 10/15/14 
 Pct Recovery = 103%  Analysis Date = 10/11/14 
 Pct Recovery = 103%  Analysis Date = 10/11/14 
 Pct Recovery = 103%  Analysis Date = 10/07/14 
 Pct Recovery = 102%  Analysis Date = 10/07/14 
 Pct Recovery = 102%  Analysis Date = 10/03/14 
 Pct Recovery = 102%  Analysis Date = 10/03/14 
 Pct Recovery = 102%  Analysis Date = 09/28/14 
 Pct Recovery = 102%  Analysis Date = 09/28/14 
 Pct Recovery = 102%  Analysis Date = 09/24/14 
 Pct Recovery = 101%  Analysis Date = 09/24/14 
 Pct Recovery = 101%  Analysis Date = 09/20/14 
 Pct Recovery = 101%  Analysis Date = 09/20/14 
 Pct Recovery = 101%  Analysis Date = 09/16/14 
 Pct Recovery = 101%  Analysis Date = 09/16/14 
 Pct Recovery = 101%  Analysis Date = 09/12/14 
 Pct Recovery = 100%  Analysis Date = 09/12/14 
 Pct Recovery = 100%  Analysis Date = 09/08/14 
 Pct Recovery = 100%  Analysis Date = 09/08/14 
 Pct Recovery = 100%  Analysis Date = 09/04/14 
 Pct Recovery = 100%  Analysis Date = 09/04/14 
 Pct Recovery = 100%  Analysis Date = 08/30/14 
 Pct Recovery = 99%  Analysis Date = 08/30/14 
 Pct Recovery = 99%  Analysis Date = 08/26/14 
 Pct Recovery = 99%  Analysis Date = 08/26/14 
 Pct Recovery = 99%  Analysis Date = 08/22/14 
 Pct Recovery = 99%  Analysis Date = 08/22/14 
 Pct Recovery = 99%  Analysis Date = 08/18/14 
 Pct Recovery = 98%  Analysis Date = 08/18/14 
 Pct Recovery = 98%  Analysis Date = 08/14/14 
 Pct Recovery = 98%  Analysis Date = 08/14/14 
 Pct Recovery = 98%  Analysis Date = 08/10/14 
 Pct Recovery = 98%  Analysis Date = 08/10/14 
 Pct Recovery = 98%  Analysis Date = 08/06/14 
 Pct Recovery = 97%  Analysis Date = 08/06/14 
 Pct Recovery = 97%  Analysis Date = 08/01/14 
 Pct Recovery = 97%  Analysis Date = 08/01/14 
 Pct Recovery = 97%  Analysis Date = 07/28/14 
 Pct Recovery = 97%  Analysis Date = 07/28/14 
 Pct Recovery = 97%  Analysis Date = 07/24/14 
 Pct Recovery = 96%  Analysis Date = 07/24/14 
 Pct Recovery = 96%  Analysis Date = 07/20/14 
 Pct Recovery = 96%  Analysis Date = 07/20/14 
 Pct Recovery = 96%  Analysis Date = 07/16/14 
 Pct Recovery = 96%  Analysis Date = 07/16/14 
 Pct Recovery = 96%  Analysis Date = 07/12/14 
 Pct Recovery = 95%  Analysis Date = 07/12/14 
 Pct Recovery = 95%  Analysis Date = 07/08/14 
 Pct Recovery = 95%  Analysis Date = 07/08/14 
 Pct Recovery = 95%  Analysis Date = 07/03/14 
 Pct Recovery = 95%  Analysis Date = 07/03/14 
 Pct Recovery = 95%  Analysis Date = 06/29/14 
 Pct Recovery = 95%  Analysis Date = 06/29/14 
 Pct Recovery = 95%  Analysis Date = 06/25/14 
 Pct Recovery = 94%  Analysis Date = 06/25/14 
 Pct Recovery = 94%  Analysis Date = 06/21/14 
 Pct Recovery = 94%  Analysis Date = 06/21/14 
 Pct Recovery = 94%  Analysis Date = 06/17/14 
 Pct Recovery = 94%  Analysis Date = 06/17/14 
 Pct Recovery = 94%  Analysis Date = 06/13/14 
 Pct Recovery = 93%  Analysis Date = 06/13/14 
 Pct Recovery = 93%  Analysis Date = 06/09/14 
 Pct Recovery = 93%  Analysis Date = 06/09/14 
 Pct Recovery = 93%  Analysis Date = 06/04/14 
 Pct Recovery = 93%  Analysis Date = 06/04/14 
 Pct Recovery = 93%  Analysis Date = 05/31/14 
 Pct Recovery = 93%  Analysis Date = 05/31/14 
 Pct Recovery = 93%  Analysis Date = 05/27/14 
 Pct Recovery = 92%  Analysis Date = 05/27/14 
 Pct Recovery = 92%  Analysis Date = 05/23/14 
 Pct Recovery = 92%  Analysis Date = 05/23/14 
 Pct Recovery = 92%  Analysis Date = 05/19/14 
 Pct Recovery = 92%  Analysis Date = 05/19/14 
 Pct Recovery = 92%  Analysis Date = 05/15/14 
 Pct Recovery = 92%  Analysis Date = 05/15/14 
 Pct Recovery = 92%  Analysis Date = 05/11/14 
 Pct Recovery = 91%  Analysis Date = 05/11/14 
 Pct Recovery = 91%  Analysis Date = 05/07/14 
 Pct Recovery = 91%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
DIMETHOXYMETHANE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 31 114% 25% 108% 27%
Total 31 114% 25% 108% 27%

Sample Statistics
DIMETHOXYMETHANE

Characteristic N % % Basis
Plotted 31 100% Spiked
Estimated Values 1 3% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 31 .  
False Negatives 0 0% 0 out of 31
Not Spiked 11 .  
False Positives 0 0% 0 out of 11

BQS OBSP Determination:
HEXACHLOROCYCLOPENTADIENE
METHOD: 4437 , TESTIDCODE: 34386GM016
Open Data Set

 Analysis Date = 07/06/16 
 SpikeMix = Accu 216041354: 40 µl & NSI 041516: 40 µl & NSI 041416HVOC: 40 µl 
 Pct Recovery = 61%  Analysis Date = 07/29/16 
 SpikeMix = Supelco LC20145V: 40 µl & NSI 041516: 40 µl & NSI 041416HVOC: 40 µl 
 Pct Recovery = 86%  Analysis Date = 08/11/16 
 SpikeMix = Phenova B20160303: 25 µl & Supelco LC20145V: 25 µl & NSI 041416HVOC: 25 µl 
 Pct Recovery = 71%  Analysis Date = 05/21/16 
 SpikeMix = Supelco LC20145V: 25 µl & NSI 041516: 25 µl & NSI 041416HVOC: 25 µl 
 Pct Recovery = 90%  Analysis Date = 07/15/14 
 SpikeMix = ChemService 2615700: 20 µl & Accu 214031128: 20 µl 
 Pct Recovery = 87%  Analysis Date = 07/03/14 
 SpikeMix = Abs 032014: 20 µl & ChemService 2615700: 20 µl 
 Pct Recovery = 77%  Analysis Date = 06/07/14 
 SpikeMix = ChemService 2615700: 20 µl & Supelco LC06437: 20 µl 
 Pct Recovery = 78%  Analysis Date = 06/06/14 
 SpikeMix = NSI 031814: 20 µl & ChemService 2615700: 20 µl 
 Pct Recovery = 67%  Analysis Date = 01/10/15 
 SpikeMix = Abs 032014: 20 µl & ERA 0321-14-05A: 20 µl 
 Pct Recovery = 82%  Analysis Date = 08/13/14 
 SpikeMix = ERA 0321-14-05: 20 µl & Accu 214031128: 20 µl 
 Pct Recovery = 76%  Analysis Date = 01/22/16 
 SpikeMix = NSI 050515HVOC: 25 µl & ERA 0601-15-05: 25 µl 
 Pct Recovery = 78%  Analysis Date = 10/09/15 
 SpikeMix = Supelco LC13544: 25 µl & NSI 050515HVOC: 25 µl 
 Pct Recovery = 72%  Analysis Date = 06/25/15 
 SpikeMix = ChemService 3818700: 25 µl & NSI 050515HVOC: 25 µl 
 Pct Recovery = 76%  Analysis Date = 08/12/16 
 SpikeMix = Accu 216041354: 15 µl & Abs 060916HVOC: 15 µl 
 Pct Recovery = 63%  Analysis Date = 07/06/16 
 SpikeMix = Phenova B20160303: 15 µl & Accu 216041354: 15 µl & NSI 041416HVOC: 15 µl 
 Pct Recovery = 55%  Analysis Date = 06/23/16 
 SpikeMix = . 
 Pct Recovery = 48%  Analysis Date = 05/20/16 
 SpikeMix = Accu 216041354: 15 µl & NSI 041516: 15 µl & Accu 216041225: 15 µl 
 Pct Recovery = 58%  Analysis Date = 07/27/16 
 SpikeMix = ChemService 5082800: 15 µl & Supelco LC20145V: 15 µl & Accu 216041225: 15 µl 
 Pct Recovery = 77%  Analysis Date = 11/25/15 
 SpikeMix = Accu 215041338: 15 µl & Abs 040315: 15 µl 
 Pct Recovery = 90%  Analysis Date = 09/24/15 
 SpikeMix = Abs 040315: 15 µl & ERA 0601-15-05: 15 µl 
 Pct Recovery = 86%  Analysis Date = 09/05/15 
 SpikeMix = Accu 215041338: 15 µl & NSI 050515HVOC: 15 µl 
 Pct Recovery = 81%  Analysis Date = 07/30/15 
 SpikeMix = Supelco LC13544: 15 µl & NSI 050515HVOC: 15 µl 
 Pct Recovery = 82%  Analysis Date = 06/16/15 
 SpikeMix = ChemService 3818700: 15 µl & NSI 050515HVOC: 15 µl 
 Pct Recovery = 82%  Analysis Date = 11/22/14 
 SpikeMix = ChemService 2615700: 10 µl & Supelco LC06437: 10 µl 
 Pct Recovery = 63%  Analysis Date = 07/30/14 
 SpikeMix = NSI 031814: 10 µl & ChemService 2615700: 10 µl 
 Pct Recovery = 72%  Analysis Date = 05/20/14 
 SpikeMix = ChemService 2615700: 10 µl & Accu 214031128: 10 µl 
 Pct Recovery = 71%  Analysis Date = 04/25/15 
 SpikeMix = Abs 032014: 10 µl & ERA 0321-14-05A: 10 µl 
 Pct Recovery = 88%  Analysis Date = 11/13/14 
 SpikeMix = ERA 0321-14-05A: 10 µl & Accu 214031128: 10 µl 
 Pct Recovery = 80%  Analysis Date = 09/06/14 
 SpikeMix = ERA 0321-14-05: 10 µl & Supelco LC06437: 10 µl 
 Pct Recovery = 107%  Analysis Date = 04/09/16 
 SpikeMix = Abs 040315: 10 µl & ChemService 3818700: 10 µl 
 Pct Recovery = 77%  Analysis Date = 01/05/16 
 SpikeMix = Accu 215041338: 10 µl & Abs 040315: 10 µl 
 Pct Recovery = 102%  Analysis Date = 10/23/15 
 SpikeMix = Abs 040315: 10 µl & ChemService 3818700: 10 µl 
 Pct Recovery = 114%  Analysis Date = 08/14/15 
 SpikeMix = Abs 040315: 10 µl & ERA 0601-15-05: 10 µl 
 Pct Recovery = 85%  Analysis Date = 05/05/15 
 SpikeMix = Supelco LC13544: 10 µl & Abs 040315: 10 µl 
 Pct Recovery = 127%  Analysis Date = 03/22/16 
 SpikeMix = Supelco LC13544: 10 µl & NSI 050515HVOC: 10 µl 
 Pct Recovery = 85%  Analysis Date = 12/05/15 
 SpikeMix = NSI 050515HVOC: 10 µl & ERA 0601-15-05: 10 µl 
 Pct Recovery = 79%  Analysis Date = 08/12/16 
 Pct Recovery = 65%  Analysis Date = 08/07/16 
 Pct Recovery = 66%  Analysis Date = 08/07/16 
 Pct Recovery = 66%  Analysis Date = 08/03/16 
 Pct Recovery = 66%  Analysis Date = 08/03/16 
 Pct Recovery = 66%  Analysis Date = 07/30/16 
 Pct Recovery = 66%  Analysis Date = 07/30/16 
 Pct Recovery = 66%  Analysis Date = 07/26/16 
 Pct Recovery = 67%  Analysis Date = 07/26/16 
 Pct Recovery = 67%  Analysis Date = 07/22/16 
 Pct Recovery = 67%  Analysis Date = 07/22/16 
 Pct Recovery = 67%  Analysis Date = 07/18/16 
 Pct Recovery = 67%  Analysis Date = 07/18/16 
 Pct Recovery = 67%  Analysis Date = 07/14/16 
 Pct Recovery = 68%  Analysis Date = 07/14/16 
 Pct Recovery = 68%  Analysis Date = 07/10/16 
 Pct Recovery = 68%  Analysis Date = 07/10/16 
 Pct Recovery = 68%  Analysis Date = 07/06/16 
 Pct Recovery = 69%  Analysis Date = 07/06/16 
 Pct Recovery = 69%  Analysis Date = 07/02/16 
 Pct Recovery = 69%  Analysis Date = 07/02/16 
 Pct Recovery = 69%  Analysis Date = 06/28/16 
 Pct Recovery = 69%  Analysis Date = 06/28/16 
 Pct Recovery = 69%  Analysis Date = 06/24/16 
 Pct Recovery = 70%  Analysis Date = 06/24/16 
 Pct Recovery = 70%  Analysis Date = 06/20/16 
 Pct Recovery = 70%  Analysis Date = 06/20/16 
 Pct Recovery = 70%  Analysis Date = 06/15/16 
 Pct Recovery = 70%  Analysis Date = 06/15/16 
 Pct Recovery = 70%  Analysis Date = 06/11/16 
 Pct Recovery = 71%  Analysis Date = 06/11/16 
 Pct Recovery = 71%  Analysis Date = 06/07/16 
 Pct Recovery = 71%  Analysis Date = 06/07/16 
 Pct Recovery = 71%  Analysis Date = 06/03/16 
 Pct Recovery = 72%  Analysis Date = 06/03/16 
 Pct Recovery = 72%  Analysis Date = 05/30/16 
 Pct Recovery = 72%  Analysis Date = 05/30/16 
 Pct Recovery = 72%  Analysis Date = 05/26/16 
 Pct Recovery = 72%  Analysis Date = 05/26/16 
 Pct Recovery = 72%  Analysis Date = 05/22/16 
 Pct Recovery = 73%  Analysis Date = 05/22/16 
 Pct Recovery = 73%  Analysis Date = 05/18/16 
 Pct Recovery = 73%  Analysis Date = 05/18/16 
 Pct Recovery = 73%  Analysis Date = 05/14/16 
 Pct Recovery = 73%  Analysis Date = 05/14/16 
 Pct Recovery = 73%  Analysis Date = 05/10/16 
 Pct Recovery = 74%  Analysis Date = 05/10/16 
 Pct Recovery = 74%  Analysis Date = 05/06/16 
 Pct Recovery = 74%  Analysis Date = 05/06/16 
 Pct Recovery = 74%  Analysis Date = 05/02/16 
 Pct Recovery = 75%  Analysis Date = 05/02/16 
 Pct Recovery = 75%  Analysis Date = 04/28/16 
 Pct Recovery = 75%  Analysis Date = 04/28/16 
 Pct Recovery = 75%  Analysis Date = 04/23/16 
 Pct Recovery = 75%  Analysis Date = 04/23/16 
 Pct Recovery = 75%  Analysis Date = 04/19/16 
 Pct Recovery = 76%  Analysis Date = 04/19/16 
 Pct Recovery = 76%  Analysis Date = 04/15/16 
 Pct Recovery = 76%  Analysis Date = 04/15/16 
 Pct Recovery = 76%  Analysis Date = 04/11/16 
 Pct Recovery = 76%  Analysis Date = 04/11/16 
 Pct Recovery = 76%  Analysis Date = 04/07/16 
 Pct Recovery = 77%  Analysis Date = 04/07/16 
 Pct Recovery = 77%  Analysis Date = 04/03/16 
 Pct Recovery = 77%  Analysis Date = 04/03/16 
 Pct Recovery = 77%  Analysis Date = 03/30/16 
 Pct Recovery = 77%  Analysis Date = 03/30/16 
 Pct Recovery = 77%  Analysis Date = 03/26/16 
 Pct Recovery = 78%  Analysis Date = 03/26/16 
 Pct Recovery = 78%  Analysis Date = 03/22/16 
 Pct Recovery = 78%  Analysis Date = 03/22/16 
 Pct Recovery = 78%  Analysis Date = 03/18/16 
 Pct Recovery = 78%  Analysis Date = 03/18/16 
 Pct Recovery = 78%  Analysis Date = 03/14/16 
 Pct Recovery = 78%  Analysis Date = 03/14/16 
 Pct Recovery = 78%  Analysis Date = 03/10/16 
 Pct Recovery = 79%  Analysis Date = 03/10/16 
 Pct Recovery = 79%  Analysis Date = 03/06/16 
 Pct Recovery = 79%  Analysis Date = 03/06/16 
 Pct Recovery = 79%  Analysis Date = 03/02/16 
 Pct Recovery = 79%  Analysis Date = 03/02/16 
 Pct Recovery = 79%  Analysis Date = 02/26/16 
 Pct Recovery = 80%  Analysis Date = 02/26/16 
 Pct Recovery = 80%  Analysis Date = 02/22/16 
 Pct Recovery = 80%  Analysis Date = 02/22/16 
 Pct Recovery = 80%  Analysis Date = 02/18/16 
 Pct Recovery = 80%  Analysis Date = 02/18/16 
 Pct Recovery = 80%  Analysis Date = 02/14/16 
 Pct Recovery = 80%  Analysis Date = 02/14/16 
 Pct Recovery = 80%  Analysis Date = 02/10/16 
 Pct Recovery = 81%  Analysis Date = 02/10/16 
 Pct Recovery = 81%  Analysis Date = 02/06/16 
 Pct Recovery = 81%  Analysis Date = 02/06/16 
 Pct Recovery = 81%  Analysis Date = 02/02/16 
 Pct Recovery = 81%  Analysis Date = 02/02/16 
 Pct Recovery = 81%  Analysis Date = 01/29/16 
 Pct Recovery = 82%  Analysis Date = 01/29/16 
 Pct Recovery = 82%  Analysis Date = 01/25/16 
 Pct Recovery = 82%  Analysis Date = 01/25/16 
 Pct Recovery = 82%  Analysis Date = 01/21/16 
 Pct Recovery = 82%  Analysis Date = 01/21/16 
 Pct Recovery = 82%  Analysis Date = 01/17/16 
 Pct Recovery = 83%  Analysis Date = 01/17/16 
 Pct Recovery = 83%  Analysis Date = 01/13/16 
 Pct Recovery = 83%  Analysis Date = 01/13/16 
 Pct Recovery = 83%  Analysis Date = 01/09/16 
 Pct Recovery = 83%  Analysis Date = 01/09/16 
 Pct Recovery = 83%  Analysis Date = 01/04/16 
 Pct Recovery = 83%  Analysis Date = 01/04/16 
 Pct Recovery = 83%  Analysis Date = 12/31/15 
 Pct Recovery = 84%  Analysis Date = 12/31/15 
 Pct Recovery = 84%  Analysis Date = 12/27/15 
 Pct Recovery = 84%  Analysis Date = 12/27/15 
 Pct Recovery = 84%  Analysis Date = 12/23/15 
 Pct Recovery = 84%  Analysis Date = 12/23/15 
 Pct Recovery = 84%  Analysis Date = 12/19/15 
 Pct Recovery = 85%  Analysis Date = 12/19/15 
 Pct Recovery = 85%  Analysis Date = 12/15/15 
 Pct Recovery = 85%  Analysis Date = 12/15/15 
 Pct Recovery = 85%  Analysis Date = 12/11/15 
 Pct Recovery = 85%  Analysis Date = 12/11/15 
 Pct Recovery = 85%  Analysis Date = 12/07/15 
 Pct Recovery = 85%  Analysis Date = 12/07/15 
 Pct Recovery = 85%  Analysis Date = 12/03/15 
 Pct Recovery = 86%  Analysis Date = 12/03/15 
 Pct Recovery = 86%  Analysis Date = 11/29/15 
 Pct Recovery = 86%  Analysis Date = 11/29/15 
 Pct Recovery = 86%  Analysis Date = 11/25/15 
 Pct Recovery = 86%  Analysis Date = 11/25/15 
 Pct Recovery = 86%  Analysis Date = 11/21/15 
 Pct Recovery = 86%  Analysis Date = 11/21/15 
 Pct Recovery = 86%  Analysis Date = 11/17/15 
 Pct Recovery = 86%  Analysis Date = 11/17/15 
 Pct Recovery = 86%  Analysis Date = 11/12/15 
 Pct Recovery = 86%  Analysis Date = 11/12/15 
 Pct Recovery = 86%  Analysis Date = 11/08/15 
 Pct Recovery = 86%  Analysis Date = 11/08/15 
 Pct Recovery = 86%  Analysis Date = 11/04/15 
 Pct Recovery = 86%  Analysis Date = 11/04/15 
 Pct Recovery = 86%  Analysis Date = 10/31/15 
 Pct Recovery = 86%  Analysis Date = 10/31/15 
 Pct Recovery = 86%  Analysis Date = 10/27/15 
 Pct Recovery = 86%  Analysis Date = 10/27/15 
 Pct Recovery = 86%  Analysis Date = 10/23/15 
 Pct Recovery = 86%  Analysis Date = 10/23/15 
 Pct Recovery = 86%  Analysis Date = 10/19/15 
 Pct Recovery = 87%  Analysis Date = 10/19/15 
 Pct Recovery = 87%  Analysis Date = 10/15/15 
 Pct Recovery = 87%  Analysis Date = 10/15/15 
 Pct Recovery = 87%  Analysis Date = 10/11/15 
 Pct Recovery = 87%  Analysis Date = 10/11/15 
 Pct Recovery = 87%  Analysis Date = 10/07/15 
 Pct Recovery = 87%  Analysis Date = 10/07/15 
 Pct Recovery = 87%  Analysis Date = 10/03/15 
 Pct Recovery = 87%  Analysis Date = 10/03/15 
 Pct Recovery = 87%  Analysis Date = 09/29/15 
 Pct Recovery = 87%  Analysis Date = 09/29/15 
 Pct Recovery = 87%  Analysis Date = 09/25/15 
 Pct Recovery = 87%  Analysis Date = 09/25/15 
 Pct Recovery = 87%  Analysis Date = 09/21/15 
 Pct Recovery = 88%  Analysis Date = 09/21/15 
 Pct Recovery = 88%  Analysis Date = 09/16/15 
 Pct Recovery = 88%  Analysis Date = 09/16/15 
 Pct Recovery = 88%  Analysis Date = 09/12/15 
 Pct Recovery = 88%  Analysis Date = 09/12/15 
 Pct Recovery = 88%  Analysis Date = 09/08/15 
 Pct Recovery = 88%  Analysis Date = 09/08/15 
 Pct Recovery = 88%  Analysis Date = 09/04/15 
 Pct Recovery = 88%  Analysis Date = 09/04/15 
 Pct Recovery = 88%  Analysis Date = 08/31/15 
 Pct Recovery = 88%  Analysis Date = 08/31/15 
 Pct Recovery = 88%  Analysis Date = 08/27/15 
 Pct Recovery = 88%  Analysis Date = 08/27/15 
 Pct Recovery = 88%  Analysis Date = 08/23/15 
 Pct Recovery = 88%  Analysis Date = 08/23/15 
 Pct Recovery = 88%  Analysis Date = 08/19/15 
 Pct Recovery = 88%  Analysis Date = 08/19/15 
 Pct Recovery = 88%  Analysis Date = 08/15/15 
 Pct Recovery = 88%  Analysis Date = 08/15/15 
 Pct Recovery = 88%  Analysis Date = 08/11/15 
 Pct Recovery = 88%  Analysis Date = 08/11/15 
 Pct Recovery = 88%  Analysis Date = 08/07/15 
 Pct Recovery = 88%  Analysis Date = 08/07/15 
 Pct Recovery = 88%  Analysis Date = 08/03/15 
 Pct Recovery = 88%  Analysis Date = 08/03/15 
 Pct Recovery = 88%  Analysis Date = 07/30/15 
 Pct Recovery = 88%  Analysis Date = 07/30/15 
 Pct Recovery = 88%  Analysis Date = 07/25/15 
 Pct Recovery = 88%  Analysis Date = 07/25/15 
 Pct Recovery = 88%  Analysis Date = 07/21/15 
 Pct Recovery = 88%  Analysis Date = 07/21/15 
 Pct Recovery = 88%  Analysis Date = 07/17/15 
 Pct Recovery = 88%  Analysis Date = 07/17/15 
 Pct Recovery = 88%  Analysis Date = 07/13/15 
 Pct Recovery = 88%  Analysis Date = 07/13/15 
 Pct Recovery = 88%  Analysis Date = 07/09/15 
 Pct Recovery = 87%  Analysis Date = 07/09/15 
 Pct Recovery = 87%  Analysis Date = 07/05/15 
 Pct Recovery = 87%  Analysis Date = 07/05/15 
 Pct Recovery = 87%  Analysis Date = 07/01/15 
 Pct Recovery = 87%  Analysis Date = 07/01/15 
 Pct Recovery = 87%  Analysis Date = 06/27/15 
 Pct Recovery = 87%  Analysis Date = 06/27/15 
 Pct Recovery = 87%  Analysis Date = 06/23/15 
 Pct Recovery = 87%  Analysis Date = 06/23/15 
 Pct Recovery = 87%  Analysis Date = 06/19/15 
 Pct Recovery = 87%  Analysis Date = 06/19/15 
 Pct Recovery = 87%  Analysis Date = 06/15/15 
 Pct Recovery = 87%  Analysis Date = 06/15/15 
 Pct Recovery = 87%  Analysis Date = 06/11/15 
 Pct Recovery = 87%  Analysis Date = 06/11/15 
 Pct Recovery = 87%  Analysis Date = 06/07/15 
 Pct Recovery = 87%  Analysis Date = 06/07/15 
 Pct Recovery = 87%  Analysis Date = 06/02/15 
 Pct Recovery = 87%  Analysis Date = 06/02/15 
 Pct Recovery = 87%  Analysis Date = 05/29/15 
 Pct Recovery = 87%  Analysis Date = 05/29/15 
 Pct Recovery = 87%  Analysis Date = 05/25/15 
 Pct Recovery = 87%  Analysis Date = 05/25/15 
 Pct Recovery = 87%  Analysis Date = 05/21/15 
 Pct Recovery = 87%  Analysis Date = 05/21/15 
 Pct Recovery = 87%  Analysis Date = 05/17/15 
 Pct Recovery = 87%  Analysis Date = 05/17/15 
 Pct Recovery = 87%  Analysis Date = 05/13/15 
 Pct Recovery = 86%  Analysis Date = 05/13/15 
 Pct Recovery = 86%  Analysis Date = 05/09/15 
 Pct Recovery = 86%  Analysis Date = 05/09/15 
 Pct Recovery = 86%  Analysis Date = 05/05/15 
 Pct Recovery = 86%  Analysis Date = 05/05/15 
 Pct Recovery = 86%  Analysis Date = 05/01/15 
 Pct Recovery = 86%  Analysis Date = 05/01/15 
 Pct Recovery = 86%  Analysis Date = 04/27/15 
 Pct Recovery = 86%  Analysis Date = 04/27/15 
 Pct Recovery = 86%  Analysis Date = 04/23/15 
 Pct Recovery = 86%  Analysis Date = 04/23/15 
 Pct Recovery = 86%  Analysis Date = 04/19/15 
 Pct Recovery = 86%  Analysis Date = 04/19/15 
 Pct Recovery = 86%  Analysis Date = 04/15/15 
 Pct Recovery = 86%  Analysis Date = 04/15/15 
 Pct Recovery = 86%  Analysis Date = 04/11/15 
 Pct Recovery = 86%  Analysis Date = 04/11/15 
 Pct Recovery = 86%  Analysis Date = 04/06/15 
 Pct Recovery = 86%  Analysis Date = 04/06/15 
 Pct Recovery = 86%  Analysis Date = 04/02/15 
 Pct Recovery = 86%  Analysis Date = 04/02/15 
 Pct Recovery = 86%  Analysis Date = 03/29/15 
 Pct Recovery = 86%  Analysis Date = 03/29/15 
 Pct Recovery = 86%  Analysis Date = 03/25/15 
 Pct Recovery = 85%  Analysis Date = 03/25/15 
 Pct Recovery = 85%  Analysis Date = 03/21/15 
 Pct Recovery = 85%  Analysis Date = 03/21/15 
 Pct Recovery = 85%  Analysis Date = 03/17/15 
 Pct Recovery = 85%  Analysis Date = 03/17/15 
 Pct Recovery = 85%  Analysis Date = 03/13/15 
 Pct Recovery = 85%  Analysis Date = 03/13/15 
 Pct Recovery = 85%  Analysis Date = 03/09/15 
 Pct Recovery = 85%  Analysis Date = 03/09/15 
 Pct Recovery = 85%  Analysis Date = 03/05/15 
 Pct Recovery = 85%  Analysis Date = 03/05/15 
 Pct Recovery = 85%  Analysis Date = 03/01/15 
 Pct Recovery = 85%  Analysis Date = 03/01/15 
 Pct Recovery = 85%  Analysis Date = 02/25/15 
 Pct Recovery = 85%  Analysis Date = 02/25/15 
 Pct Recovery = 85%  Analysis Date = 02/21/15 
 Pct Recovery = 85%  Analysis Date = 02/21/15 
 Pct Recovery = 85%  Analysis Date = 02/17/15 
 Pct Recovery = 85%  Analysis Date = 02/17/15 
 Pct Recovery = 85%  Analysis Date = 02/12/15 
 Pct Recovery = 85%  Analysis Date = 02/12/15 
 Pct Recovery = 85%  Analysis Date = 02/08/15 
 Pct Recovery = 85%  Analysis Date = 02/08/15 
 Pct Recovery = 85%  Analysis Date = 02/04/15 
 Pct Recovery = 84%  Analysis Date = 02/04/15 
 Pct Recovery = 84%  Analysis Date = 01/31/15 
 Pct Recovery = 84%  Analysis Date = 01/31/15 
 Pct Recovery = 84%  Analysis Date = 01/27/15 
 Pct Recovery = 84%  Analysis Date = 01/27/15 
 Pct Recovery = 84%  Analysis Date = 01/23/15 
 Pct Recovery = 84%  Analysis Date = 01/23/15 
 Pct Recovery = 84%  Analysis Date = 01/19/15 
 Pct Recovery = 84%  Analysis Date = 01/19/15 
 Pct Recovery = 84%  Analysis Date = 01/15/15 
 Pct Recovery = 84%  Analysis Date = 01/15/15 
 Pct Recovery = 84%  Analysis Date = 01/11/15 
 Pct Recovery = 84%  Analysis Date = 01/11/15 
 Pct Recovery = 84%  Analysis Date = 01/07/15 
 Pct Recovery = 84%  Analysis Date = 01/07/15 
 Pct Recovery = 84%  Analysis Date = 01/03/15 
 Pct Recovery = 84%  Analysis Date = 01/03/15 
 Pct Recovery = 84%  Analysis Date = 12/30/14 
 Pct Recovery = 84%  Analysis Date = 12/30/14 
 Pct Recovery = 84%  Analysis Date = 12/26/14 
 Pct Recovery = 84%  Analysis Date = 12/26/14 
 Pct Recovery = 84%  Analysis Date = 12/21/14 
 Pct Recovery = 84%  Analysis Date = 12/21/14 
 Pct Recovery = 84%  Analysis Date = 12/17/14 
 Pct Recovery = 84%  Analysis Date = 12/17/14 
 Pct Recovery = 84%  Analysis Date = 12/13/14 
 Pct Recovery = 83%  Analysis Date = 12/13/14 
 Pct Recovery = 83%  Analysis Date = 12/09/14 
 Pct Recovery = 83%  Analysis Date = 12/09/14 
 Pct Recovery = 83%  Analysis Date = 12/05/14 
 Pct Recovery = 83%  Analysis Date = 12/05/14 
 Pct Recovery = 83%  Analysis Date = 12/01/14 
 Pct Recovery = 83%  Analysis Date = 12/01/14 
 Pct Recovery = 83%  Analysis Date = 11/27/14 
 Pct Recovery = 83%  Analysis Date = 11/27/14 
 Pct Recovery = 83%  Analysis Date = 11/23/14 
 Pct Recovery = 83%  Analysis Date = 11/23/14 
 Pct Recovery = 83%  Analysis Date = 11/19/14 
 Pct Recovery = 83%  Analysis Date = 11/19/14 
 Pct Recovery = 83%  Analysis Date = 11/15/14 
 Pct Recovery = 83%  Analysis Date = 11/15/14 
 Pct Recovery = 83%  Analysis Date = 11/11/14 
 Pct Recovery = 83%  Analysis Date = 11/11/14 
 Pct Recovery = 83%  Analysis Date = 11/07/14 
 Pct Recovery = 83%  Analysis Date = 11/07/14 
 Pct Recovery = 83%  Analysis Date = 11/03/14 
 Pct Recovery = 82%  Analysis Date = 11/03/14 
 Pct Recovery = 82%  Analysis Date = 10/30/14 
 Pct Recovery = 82%  Analysis Date = 10/30/14 
 Pct Recovery = 82%  Analysis Date = 10/25/14 
 Pct Recovery = 82%  Analysis Date = 10/25/14 
 Pct Recovery = 82%  Analysis Date = 10/21/14 
 Pct Recovery = 82%  Analysis Date = 10/21/14 
 Pct Recovery = 82%  Analysis Date = 10/17/14 
 Pct Recovery = 82%  Analysis Date = 10/17/14 
 Pct Recovery = 82%  Analysis Date = 10/13/14 
 Pct Recovery = 81%  Analysis Date = 10/13/14 
 Pct Recovery = 81%  Analysis Date = 10/09/14 
 Pct Recovery = 81%  Analysis Date = 10/09/14 
 Pct Recovery = 81%  Analysis Date = 10/05/14 
 Pct Recovery = 81%  Analysis Date = 10/05/14 
 Pct Recovery = 81%  Analysis Date = 10/01/14 
 Pct Recovery = 81%  Analysis Date = 10/01/14 
 Pct Recovery = 81%  Analysis Date = 09/27/14 
 Pct Recovery = 81%  Analysis Date = 09/27/14 
 Pct Recovery = 81%  Analysis Date = 09/23/14 
 Pct Recovery = 81%  Analysis Date = 09/23/14 
 Pct Recovery = 81%  Analysis Date = 09/19/14 
 Pct Recovery = 80%  Analysis Date = 09/19/14 
 Pct Recovery = 80%  Analysis Date = 09/15/14 
 Pct Recovery = 80%  Analysis Date = 09/15/14 
 Pct Recovery = 80%  Analysis Date = 09/11/14 
 Pct Recovery = 80%  Analysis Date = 09/11/14 
 Pct Recovery = 80%  Analysis Date = 09/07/14 
 Pct Recovery = 80%  Analysis Date = 09/07/14 
 Pct Recovery = 80%  Analysis Date = 09/02/14 
 Pct Recovery = 80%  Analysis Date = 09/02/14 
 Pct Recovery = 80%  Analysis Date = 08/29/14 
 Pct Recovery = 80%  Analysis Date = 08/29/14 
 Pct Recovery = 80%  Analysis Date = 08/25/14 
 Pct Recovery = 79%  Analysis Date = 08/25/14 
 Pct Recovery = 79%  Analysis Date = 08/21/14 
 Pct Recovery = 79%  Analysis Date = 08/21/14 
 Pct Recovery = 79%  Analysis Date = 08/17/14 
 Pct Recovery = 79%  Analysis Date = 08/17/14 
 Pct Recovery = 79%  Analysis Date = 08/13/14 
 Pct Recovery = 79%  Analysis Date = 08/13/14 
 Pct Recovery = 79%  Analysis Date = 08/09/14 
 Pct Recovery = 79%  Analysis Date = 08/09/14 
 Pct Recovery = 79%  Analysis Date = 08/05/14 
 Pct Recovery = 78%  Analysis Date = 08/05/14 
 Pct Recovery = 78%  Analysis Date = 08/01/14 
 Pct Recovery = 78%  Analysis Date = 08/01/14 
 Pct Recovery = 78%  Analysis Date = 07/28/14 
 Pct Recovery = 78%  Analysis Date = 07/28/14 
 Pct Recovery = 78%  Analysis Date = 07/24/14 
 Pct Recovery = 78%  Analysis Date = 07/24/14 
 Pct Recovery = 78%  Analysis Date = 07/20/14 
 Pct Recovery = 78%  Analysis Date = 07/20/14 
 Pct Recovery = 78%  Analysis Date = 07/16/14 
 Pct Recovery = 78%  Analysis Date = 07/16/14 
 Pct Recovery = 78%  Analysis Date = 07/11/14 
 Pct Recovery = 77%  Analysis Date = 07/11/14 
 Pct Recovery = 77%  Analysis Date = 07/07/14 
 Pct Recovery = 77%  Analysis Date = 07/07/14 
 Pct Recovery = 77%  Analysis Date = 07/03/14 
 Pct Recovery = 77%  Analysis Date = 07/03/14 
 Pct Recovery = 77%  Analysis Date = 06/29/14 
 Pct Recovery = 77%  Analysis Date = 06/29/14 
 Pct Recovery = 77%  Analysis Date = 06/25/14 
 Pct Recovery = 77%  Analysis Date = 06/25/14 
 Pct Recovery = 77%  Analysis Date = 06/21/14 
 Pct Recovery = 76%  Analysis Date = 06/21/14 
 Pct Recovery = 76%  Analysis Date = 06/17/14 
 Pct Recovery = 76%  Analysis Date = 06/17/14 
 Pct Recovery = 76%  Analysis Date = 06/13/14 
 Pct Recovery = 76%  Analysis Date = 06/13/14 
 Pct Recovery = 76%  Analysis Date = 06/09/14 
 Pct Recovery = 76%  Analysis Date = 06/09/14 
 Pct Recovery = 76%  Analysis Date = 06/05/14 
 Pct Recovery = 76%  Analysis Date = 06/05/14 
 Pct Recovery = 76%  Analysis Date = 06/01/14 
 Pct Recovery = 76%  Analysis Date = 06/01/14 
 Pct Recovery = 76%  Analysis Date = 05/28/14 
 Pct Recovery = 75%  Analysis Date = 05/28/14 
 Pct Recovery = 75%  Analysis Date = 05/24/14 
 Pct Recovery = 75%  Analysis Date = 05/24/14 
 Pct Recovery = 75%  Analysis Date = 05/20/14 
 Pct Recovery = 75%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
HEXACHLOROCYCLOPENTADIENE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 36 80% 16% 78% 11%
Total 36 80% 16% 78% 11%

Sample Statistics
HEXACHLOROCYCLOPENTADIENE

Characteristic N % % Basis
Plotted 36 100% Spiked
Estimated Values 36 100% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 36 .  
False Negatives 0 0% 0 out of 36
Not Spiked 19 .  
False Positives 0 0% 0 out of 19

BQS OBSP Determination:
HEXANOL, 2-ETHYL-
METHOD: 4437 , TESTIDCODE: 77311GM016
Open Data Set

 Analysis Date = 07/29/16 
 SpikeMix = Supelco LC20145V: 40 µl & NSI 041516: 40 µl & NSI 041416HVOC: 40 µl 
 Pct Recovery = 76%  Analysis Date = 07/06/16 
 SpikeMix = Accu 216041354: 40 µl & NSI 041516: 40 µl & NSI 041416HVOC: 40 µl 
 Pct Recovery = 69%  Analysis Date = 06/29/16 
 SpikeMix = NSI 041516: 40 µl & ChemService 5082800: 40 µl 
 Pct Recovery = 74%  Analysis Date = 07/14/16 
 SpikeMix = NSI 041516: 25 µl & ChemService 5082800: 25 µl & NSI 041416HVOC: 25 µl 
 Pct Recovery = 62%  Analysis Date = 05/21/16 
 SpikeMix = Supelco LC20145V: 25 µl & NSI 041516: 25 µl & NSI 041416HVOC: 25 µl 
 Pct Recovery = 80%  Analysis Date = 03/19/15 
 SpikeMix = Supelco LC06437: 20 µl & NSI 031814: 20 µl 
 Pct Recovery = 100%  Analysis Date = 03/19/15 
 SpikeMix = Supelco LC06437: 20 µl & NSI 031814: 20 µl 
 Pct Recovery = 100%  Analysis Date = 06/06/14 
 SpikeMix = NSI 031814: 20 µl & ChemService 2615700: 20 µl 
 Pct Recovery = 95%  Analysis Date = 06/06/14 
 SpikeMix = NSI 031814: 20 µl & ChemService 2615700: 20 µl 
 Pct Recovery = 95%  Analysis Date = 05/07/14 
 SpikeMix = NSI 031814: 20 µl & Accu 214031128: 20 µl 
 Pct Recovery = 92%  Analysis Date = 05/07/14 
 SpikeMix = NSI 031814: 20 µl & Accu 214031128: 20 µl 
 Pct Recovery = 92%  Analysis Date = 01/10/15 
 SpikeMix = Abs 032014: 20 µl & ERA 0321-14-05A: 20 µl 
 Pct Recovery = 85%  Analysis Date = 01/10/15 
 SpikeMix = Abs 032014: 20 µl & ERA 0321-14-05A: 20 µl 
 Pct Recovery = 85%  Analysis Date = 08/20/14 
 SpikeMix = Supelco LC06437: 20 µl & Abs 032014: 20 µl 
 Pct Recovery = 106%  Analysis Date = 08/20/14 
 SpikeMix = Supelco LC06437: 20 µl & Abs 032014: 20 µl 
 Pct Recovery = 106%  Analysis Date = 07/23/14 
 SpikeMix = Accu 214031128: 20 µl & Abs 032014: 20 µl 
 Pct Recovery = 106%  Analysis Date = 07/23/14 
 SpikeMix = Accu 214031128: 20 µl & Abs 032014: 20 µl 
 Pct Recovery = 106%  Analysis Date = 07/03/14 
 SpikeMix = Abs 032014: 20 µl & ChemService 2615700: 20 µl 
 Pct Recovery = 104%  Analysis Date = 07/03/14 
 SpikeMix = Abs 032014: 20 µl & ChemService 2615700: 20 µl 
 Pct Recovery = 104%  Analysis Date = 10/09/15 
 SpikeMix = Supelco LC13544: 25 µl & NSI 050515HVOC: 25 µl 
 Pct Recovery = 91%  Analysis Date = 10/09/15 
 SpikeMix = ERA 0601-15-05: 25 µl & Accu 215041338: 25 µl 
 Pct Recovery = 88%  Analysis Date = 06/26/15 
 SpikeMix = ChemService 3818700: 25 µl & Accu 215041338: 25 µl 
 Pct Recovery = 81%  Analysis Date = 08/12/16 
 SpikeMix = Accu 216041354: 15 µl & Abs 060916HVOC: 15 µl 
 Pct Recovery = 92%  Analysis Date = 06/03/16 
 SpikeMix = NSI 041516: 15 µl & Phenova B20160303: 15 µl & NSI 041416HVOC: 15 µl 
 Pct Recovery = 88%  Analysis Date = 05/20/16 
 SpikeMix = Accu 216041354: 15 µl & NSI 041516: 15 µl & Accu 216041225: 15 µl 
 Pct Recovery = 88%  Analysis Date = 04/28/16 
 SpikeMix = ChemService 3818700: 15 µl & Supelco LC13544: 15 µl 
 Pct Recovery = 102%  Analysis Date = 08/24/15 
 SpikeMix = ERA 0601-15-05: 15 µl & Supelco LC13544: 15 µl 
 Pct Recovery = 104%  Analysis Date = 07/30/15 
 SpikeMix = Supelco LC13544: 15 µl & NSI 050515HVOC: 15 µl 
 Pct Recovery = 89%  Analysis Date = 05/14/15 
 SpikeMix = ChemService 3818700: 15 µl & Supelco LC13544: 15 µl 
 Pct Recovery = 100%  Analysis Date = 11/25/15 
 SpikeMix = Accu 215041338: 15 µl & Abs 040315: 15 µl 
 Pct Recovery = 94%  Analysis Date = 09/05/15 
 SpikeMix = Accu 215041338: 15 µl & NSI 050515HVOC: 15 µl 
 Pct Recovery = 89%  Analysis Date = 12/13/14 
 SpikeMix = Accu 214031128: 10 µl & NSI 031814: 10 µl 
 Pct Recovery = 100%  Analysis Date = 12/13/14 
 SpikeMix = Accu 214031128: 10 µl & NSI 031814: 10 µl 
 Pct Recovery = 100%  Analysis Date = 07/30/14 
 SpikeMix = NSI 031814: 10 µl & ChemService 2615700: 10 µl 
 Pct Recovery = 125%  Analysis Date = 07/30/14 
 SpikeMix = NSI 031814: 10 µl & ChemService 2615700: 10 µl 
 Pct Recovery = 125%  Analysis Date = 04/25/15 
 SpikeMix = Abs 032014: 10 µl & ERA 0321-14-05A: 10 µl 
 Pct Recovery = 97%  Analysis Date = 09/11/14 
 SpikeMix = Accu 214031128: 10 µl & Abs 032014: 10 µl 
 Pct Recovery = 87%  Analysis Date = 09/11/14 
 SpikeMix = Accu 214031128: 10 µl & Abs 032014: 10 µl 
 Pct Recovery = 87%  Analysis Date = 06/17/14 
 SpikeMix = Supelco LC06437: 10 µl & Abs 032014: 10 µl 
 Pct Recovery = 142%  Analysis Date = 06/17/14 
 SpikeMix = Supelco LC06437: 10 µl & Abs 032014: 10 µl 
 Pct Recovery = 142%  Analysis Date = 03/22/16 
 SpikeMix = Supelco LC13544: 10 µl & NSI 050515HVOC: 10 µl 
 Pct Recovery = 93%  Analysis Date = 12/10/15 
 SpikeMix = ChemService 3818700: 10 µl & Supelco LC13544: 10 µl 
 Pct Recovery = 100%  Analysis Date = 05/05/15 
 SpikeMix = Supelco LC13544: 10 µl & Abs 040315: 10 µl 
 Pct Recovery = 103%  Analysis Date = 02/12/16 
 SpikeMix = ERA 0601-15-05: 10 µl & Accu 215041338: 10 µl 
 Pct Recovery = 97%  Analysis Date = 01/05/16 
 SpikeMix = Accu 215041338: 10 µl & Abs 040315: 10 µl 
 Pct Recovery = 104%  Analysis Date = 05/20/15 
 SpikeMix = ChemService 3818700: 10 µl & Accu 215041338: 10 µl 
 Pct Recovery = 114%  Analysis Date = 08/11/16 
 Pct Recovery = 80%  Analysis Date = 08/07/16 
 Pct Recovery = 80%  Analysis Date = 08/07/16 
 Pct Recovery = 80%  Analysis Date = 08/03/16 
 Pct Recovery = 80%  Analysis Date = 08/03/16 
 Pct Recovery = 80%  Analysis Date = 07/30/16 
 Pct Recovery = 80%  Analysis Date = 07/30/16 
 Pct Recovery = 80%  Analysis Date = 07/26/16 
 Pct Recovery = 81%  Analysis Date = 07/26/16 
 Pct Recovery = 81%  Analysis Date = 07/22/16 
 Pct Recovery = 81%  Analysis Date = 07/22/16 
 Pct Recovery = 81%  Analysis Date = 07/18/16 
 Pct Recovery = 81%  Analysis Date = 07/18/16 
 Pct Recovery = 81%  Analysis Date = 07/14/16 
 Pct Recovery = 81%  Analysis Date = 07/14/16 
 Pct Recovery = 81%  Analysis Date = 07/09/16 
 Pct Recovery = 82%  Analysis Date = 07/09/16 
 Pct Recovery = 82%  Analysis Date = 07/05/16 
 Pct Recovery = 82%  Analysis Date = 07/05/16 
 Pct Recovery = 82%  Analysis Date = 07/01/16 
 Pct Recovery = 82%  Analysis Date = 07/01/16 
 Pct Recovery = 82%  Analysis Date = 06/27/16 
 Pct Recovery = 82%  Analysis Date = 06/27/16 
 Pct Recovery = 82%  Analysis Date = 06/23/16 
 Pct Recovery = 82%  Analysis Date = 06/23/16 
 Pct Recovery = 82%  Analysis Date = 06/19/16 
 Pct Recovery = 83%  Analysis Date = 06/19/16 
 Pct Recovery = 83%  Analysis Date = 06/15/16 
 Pct Recovery = 83%  Analysis Date = 06/15/16 
 Pct Recovery = 83%  Analysis Date = 06/10/16 
 Pct Recovery = 83%  Analysis Date = 06/10/16 
 Pct Recovery = 83%  Analysis Date = 06/06/16 
 Pct Recovery = 83%  Analysis Date = 06/06/16 
 Pct Recovery = 83%  Analysis Date = 06/02/16 
 Pct Recovery = 84%  Analysis Date = 06/02/16 
 Pct Recovery = 84%  Analysis Date = 05/29/16 
 Pct Recovery = 84%  Analysis Date = 05/29/16 
 Pct Recovery = 84%  Analysis Date = 05/25/16 
 Pct Recovery = 84%  Analysis Date = 05/25/16 
 Pct Recovery = 84%  Analysis Date = 05/21/16 
 Pct Recovery = 84%  Analysis Date = 05/21/16 
 Pct Recovery = 84%  Analysis Date = 05/17/16 
 Pct Recovery = 84%  Analysis Date = 05/17/16 
 Pct Recovery = 84%  Analysis Date = 05/12/16 
 Pct Recovery = 85%  Analysis Date = 05/12/16 
 Pct Recovery = 85%  Analysis Date = 05/08/16 
 Pct Recovery = 85%  Analysis Date = 05/08/16 
 Pct Recovery = 85%  Analysis Date = 05/04/16 
 Pct Recovery = 85%  Analysis Date = 05/04/16 
 Pct Recovery = 85%  Analysis Date = 04/30/16 
 Pct Recovery = 85%  Analysis Date = 04/30/16 
 Pct Recovery = 85%  Analysis Date = 04/26/16 
 Pct Recovery = 85%  Analysis Date = 04/26/16 
 Pct Recovery = 85%  Analysis Date = 04/22/16 
 Pct Recovery = 86%  Analysis Date = 04/22/16 
 Pct Recovery = 86%  Analysis Date = 04/18/16 
 Pct Recovery = 86%  Analysis Date = 04/18/16 
 Pct Recovery = 86%  Analysis Date = 04/13/16 
 Pct Recovery = 86%  Analysis Date = 04/13/16 
 Pct Recovery = 86%  Analysis Date = 04/09/16 
 Pct Recovery = 86%  Analysis Date = 04/09/16 
 Pct Recovery = 86%  Analysis Date = 04/05/16 
 Pct Recovery = 86%  Analysis Date = 04/05/16 
 Pct Recovery = 86%  Analysis Date = 04/01/16 
 Pct Recovery = 87%  Analysis Date = 04/01/16 
 Pct Recovery = 87%  Analysis Date = 03/28/16 
 Pct Recovery = 87%  Analysis Date = 03/28/16 
 Pct Recovery = 87%  Analysis Date = 03/24/16 
 Pct Recovery = 87%  Analysis Date = 03/24/16 
 Pct Recovery = 87%  Analysis Date = 03/20/16 
 Pct Recovery = 87%  Analysis Date = 03/20/16 
 Pct Recovery = 87%  Analysis Date = 03/15/16 
 Pct Recovery = 87%  Analysis Date = 03/15/16 
 Pct Recovery = 87%  Analysis Date = 03/11/16 
 Pct Recovery = 88%  Analysis Date = 03/11/16 
 Pct Recovery = 88%  Analysis Date = 03/07/16 
 Pct Recovery = 88%  Analysis Date = 03/07/16 
 Pct Recovery = 88%  Analysis Date = 03/03/16 
 Pct Recovery = 88%  Analysis Date = 03/03/16 
 Pct Recovery = 88%  Analysis Date = 02/28/16 
 Pct Recovery = 88%  Analysis Date = 02/28/16 
 Pct Recovery = 88%  Analysis Date = 02/24/16 
 Pct Recovery = 88%  Analysis Date = 02/24/16 
 Pct Recovery = 88%  Analysis Date = 02/20/16 
 Pct Recovery = 89%  Analysis Date = 02/20/16 
 Pct Recovery = 89%  Analysis Date = 02/15/16 
 Pct Recovery = 89%  Analysis Date = 02/15/16 
 Pct Recovery = 89%  Analysis Date = 02/11/16 
 Pct Recovery = 89%  Analysis Date = 02/11/16 
 Pct Recovery = 89%  Analysis Date = 02/07/16 
 Pct Recovery = 89%  Analysis Date = 02/07/16 
 Pct Recovery = 89%  Analysis Date = 02/03/16 
 Pct Recovery = 89%  Analysis Date = 02/03/16 
 Pct Recovery = 89%  Analysis Date = 01/30/16 
 Pct Recovery = 90%  Analysis Date = 01/30/16 
 Pct Recovery = 90%  Analysis Date = 01/26/16 
 Pct Recovery = 90%  Analysis Date = 01/26/16 
 Pct Recovery = 90%  Analysis Date = 01/22/16 
 Pct Recovery = 90%  Analysis Date = 01/22/16 
 Pct Recovery = 90%  Analysis Date = 01/17/16 
 Pct Recovery = 90%  Analysis Date = 01/17/16 
 Pct Recovery = 90%  Analysis Date = 01/13/16 
 Pct Recovery = 90%  Analysis Date = 01/13/16 
 Pct Recovery = 90%  Analysis Date = 01/09/16 
 Pct Recovery = 91%  Analysis Date = 01/09/16 
 Pct Recovery = 91%  Analysis Date = 01/05/16 
 Pct Recovery = 91%  Analysis Date = 01/05/16 
 Pct Recovery = 91%  Analysis Date = 01/01/16 
 Pct Recovery = 91%  Analysis Date = 01/01/16 
 Pct Recovery = 91%  Analysis Date = 12/28/15 
 Pct Recovery = 91%  Analysis Date = 12/28/15 
 Pct Recovery = 91%  Analysis Date = 12/24/15 
 Pct Recovery = 92%  Analysis Date = 12/24/15 
 Pct Recovery = 92%  Analysis Date = 12/20/15 
 Pct Recovery = 92%  Analysis Date = 12/20/15 
 Pct Recovery = 92%  Analysis Date = 12/15/15 
 Pct Recovery = 92%  Analysis Date = 12/15/15 
 Pct Recovery = 92%  Analysis Date = 12/11/15 
 Pct Recovery = 92%  Analysis Date = 12/11/15 
 Pct Recovery = 92%  Analysis Date = 12/07/15 
 Pct Recovery = 92%  Analysis Date = 12/07/15 
 Pct Recovery = 92%  Analysis Date = 12/03/15 
 Pct Recovery = 93%  Analysis Date = 12/03/15 
 Pct Recovery = 93%  Analysis Date = 11/29/15 
 Pct Recovery = 93%  Analysis Date = 11/29/15 
 Pct Recovery = 93%  Analysis Date = 11/25/15 
 Pct Recovery = 93%  Analysis Date = 11/25/15 
 Pct Recovery = 93%  Analysis Date = 11/21/15 
 Pct Recovery = 93%  Analysis Date = 11/21/15 
 Pct Recovery = 93%  Analysis Date = 11/16/15 
 Pct Recovery = 93%  Analysis Date = 11/16/15 
 Pct Recovery = 93%  Analysis Date = 11/12/15 
 Pct Recovery = 94%  Analysis Date = 11/12/15 
 Pct Recovery = 94%  Analysis Date = 11/08/15 
 Pct Recovery = 94%  Analysis Date = 11/08/15 
 Pct Recovery = 94%  Analysis Date = 11/04/15 
 Pct Recovery = 94%  Analysis Date = 11/04/15 
 Pct Recovery = 94%  Analysis Date = 10/31/15 
 Pct Recovery = 94%  Analysis Date = 10/31/15 
 Pct Recovery = 94%  Analysis Date = 10/27/15 
 Pct Recovery = 94%  Analysis Date = 10/27/15 
 Pct Recovery = 94%  Analysis Date = 10/23/15 
 Pct Recovery = 95%  Analysis Date = 10/23/15 
 Pct Recovery = 95%  Analysis Date = 10/18/15 
 Pct Recovery = 95%  Analysis Date = 10/18/15 
 Pct Recovery = 95%  Analysis Date = 10/14/15 
 Pct Recovery = 95%  Analysis Date = 10/14/15 
 Pct Recovery = 95%  Analysis Date = 10/10/15 
 Pct Recovery = 95%  Analysis Date = 10/10/15 
 Pct Recovery = 95%  Analysis Date = 10/06/15 
 Pct Recovery = 95%  Analysis Date = 10/06/15 
 Pct Recovery = 95%  Analysis Date = 10/02/15 
 Pct Recovery = 96%  Analysis Date = 10/02/15 
 Pct Recovery = 96%  Analysis Date = 09/28/15 
 Pct Recovery = 96%  Analysis Date = 09/28/15 
 Pct Recovery = 96%  Analysis Date = 09/24/15 
 Pct Recovery = 96%  Analysis Date = 09/24/15 
 Pct Recovery = 96%  Analysis Date = 09/19/15 
 Pct Recovery = 96%  Analysis Date = 09/19/15 
 Pct Recovery = 96%  Analysis Date = 09/15/15 
 Pct Recovery = 96%  Analysis Date = 09/15/15 
 Pct Recovery = 96%  Analysis Date = 09/11/15 
 Pct Recovery = 96%  Analysis Date = 09/11/15 
 Pct Recovery = 96%  Analysis Date = 09/07/15 
 Pct Recovery = 96%  Analysis Date = 09/07/15 
 Pct Recovery = 96%  Analysis Date = 09/03/15 
 Pct Recovery = 96%  Analysis Date = 09/03/15 
 Pct Recovery = 96%  Analysis Date = 08/30/15 
 Pct Recovery = 96%  Analysis Date = 08/30/15 
 Pct Recovery = 96%  Analysis Date = 08/26/15 
 Pct Recovery = 96%  Analysis Date = 08/26/15 
 Pct Recovery = 96%  Analysis Date = 08/21/15 
 Pct Recovery = 96%  Analysis Date = 08/21/15 
 Pct Recovery = 96%  Analysis Date = 08/17/15 
 Pct Recovery = 96%  Analysis Date = 08/17/15 
 Pct Recovery = 96%  Analysis Date = 08/13/15 
 Pct Recovery = 96%  Analysis Date = 08/13/15 
 Pct Recovery = 96%  Analysis Date = 08/09/15 
 Pct Recovery = 96%  Analysis Date = 08/09/15 
 Pct Recovery = 96%  Analysis Date = 08/05/15 
 Pct Recovery = 96%  Analysis Date = 08/05/15 
 Pct Recovery = 96%  Analysis Date = 08/01/15 
 Pct Recovery = 96%  Analysis Date = 08/01/15 
 Pct Recovery = 96%  Analysis Date = 07/28/15 
 Pct Recovery = 96%  Analysis Date = 07/28/15 
 Pct Recovery = 96%  Analysis Date = 07/23/15 
 Pct Recovery = 96%  Analysis Date = 07/23/15 
 Pct Recovery = 96%  Analysis Date = 07/19/15 
 Pct Recovery = 96%  Analysis Date = 07/19/15 
 Pct Recovery = 96%  Analysis Date = 07/15/15 
 Pct Recovery = 96%  Analysis Date = 07/15/15 
 Pct Recovery = 96%  Analysis Date = 07/11/15 
 Pct Recovery = 96%  Analysis Date = 07/11/15 
 Pct Recovery = 96%  Analysis Date = 07/07/15 
 Pct Recovery = 96%  Analysis Date = 07/07/15 
 Pct Recovery = 96%  Analysis Date = 07/03/15 
 Pct Recovery = 96%  Analysis Date = 07/03/15 
 Pct Recovery = 96%  Analysis Date = 06/29/15 
 Pct Recovery = 96%  Analysis Date = 06/29/15 
 Pct Recovery = 96%  Analysis Date = 06/24/15 
 Pct Recovery = 96%  Analysis Date = 06/24/15 
 Pct Recovery = 96%  Analysis Date = 06/20/15 
 Pct Recovery = 96%  Analysis Date = 06/20/15 
 Pct Recovery = 96%  Analysis Date = 06/16/15 
 Pct Recovery = 96%  Analysis Date = 06/16/15 
 Pct Recovery = 96%  Analysis Date = 06/12/15 
 Pct Recovery = 96%  Analysis Date = 06/12/15 
 Pct Recovery = 96%  Analysis Date = 06/08/15 
 Pct Recovery = 96%  Analysis Date = 06/08/15 
 Pct Recovery = 96%  Analysis Date = 06/04/15 
 Pct Recovery = 96%  Analysis Date = 06/04/15 
 Pct Recovery = 96%  Analysis Date = 05/31/15 
 Pct Recovery = 96%  Analysis Date = 05/31/15 
 Pct Recovery = 96%  Analysis Date = 05/27/15 
 Pct Recovery = 96%  Analysis Date = 05/27/15 
 Pct Recovery = 96%  Analysis Date = 05/22/15 
 Pct Recovery = 96%  Analysis Date = 05/22/15 
 Pct Recovery = 96%  Analysis Date = 05/18/15 
 Pct Recovery = 96%  Analysis Date = 05/18/15 
 Pct Recovery = 96%  Analysis Date = 05/14/15 
 Pct Recovery = 96%  Analysis Date = 05/14/15 
 Pct Recovery = 96%  Analysis Date = 05/10/15 
 Pct Recovery = 96%  Analysis Date = 05/10/15 
 Pct Recovery = 96%  Analysis Date = 05/06/15 
 Pct Recovery = 96%  Analysis Date = 05/06/15 
 Pct Recovery = 96%  Analysis Date = 05/02/15 
 Pct Recovery = 96%  Analysis Date = 05/02/15 
 Pct Recovery = 96%  Analysis Date = 04/28/15 
 Pct Recovery = 96%  Analysis Date = 04/28/15 
 Pct Recovery = 96%  Analysis Date = 04/23/15 
 Pct Recovery = 96%  Analysis Date = 04/23/15 
 Pct Recovery = 96%  Analysis Date = 04/19/15 
 Pct Recovery = 96%  Analysis Date = 04/19/15 
 Pct Recovery = 96%  Analysis Date = 04/15/15 
 Pct Recovery = 96%  Analysis Date = 04/15/15 
 Pct Recovery = 96%  Analysis Date = 04/11/15 
 Pct Recovery = 96%  Analysis Date = 04/11/15 
 Pct Recovery = 96%  Analysis Date = 04/07/15 
 Pct Recovery = 96%  Analysis Date = 04/07/15 
 Pct Recovery = 96%  Analysis Date = 04/03/15 
 Pct Recovery = 96%  Analysis Date = 04/03/15 
 Pct Recovery = 96%  Analysis Date = 03/30/15 
 Pct Recovery = 97%  Analysis Date = 03/30/15 
 Pct Recovery = 97%  Analysis Date = 03/25/15 
 Pct Recovery = 97%  Analysis Date = 03/25/15 
 Pct Recovery = 97%  Analysis Date = 03/21/15 
 Pct Recovery = 97%  Analysis Date = 03/21/15 
 Pct Recovery = 97%  Analysis Date = 03/17/15 
 Pct Recovery = 97%  Analysis Date = 03/17/15 
 Pct Recovery = 97%  Analysis Date = 03/13/15 
 Pct Recovery = 97%  Analysis Date = 03/13/15 
 Pct Recovery = 97%  Analysis Date = 03/09/15 
 Pct Recovery = 97%  Analysis Date = 03/09/15 
 Pct Recovery = 97%  Analysis Date = 03/05/15 
 Pct Recovery = 97%  Analysis Date = 03/05/15 
 Pct Recovery = 97%  Analysis Date = 03/01/15 
 Pct Recovery = 97%  Analysis Date = 03/01/15 
 Pct Recovery = 97%  Analysis Date = 02/24/15 
 Pct Recovery = 97%  Analysis Date = 02/24/15 
 Pct Recovery = 97%  Analysis Date = 02/20/15 
 Pct Recovery = 97%  Analysis Date = 02/20/15 
 Pct Recovery = 97%  Analysis Date = 02/16/15 
 Pct Recovery = 97%  Analysis Date = 02/16/15 
 Pct Recovery = 97%  Analysis Date = 02/12/15 
 Pct Recovery = 98%  Analysis Date = 02/12/15 
 Pct Recovery = 98%  Analysis Date = 02/08/15 
 Pct Recovery = 98%  Analysis Date = 02/08/15 
 Pct Recovery = 98%  Analysis Date = 02/04/15 
 Pct Recovery = 98%  Analysis Date = 02/04/15 
 Pct Recovery = 98%  Analysis Date = 01/31/15 
 Pct Recovery = 98%  Analysis Date = 01/31/15 
 Pct Recovery = 98%  Analysis Date = 01/26/15 
 Pct Recovery = 98%  Analysis Date = 01/26/15 
 Pct Recovery = 98%  Analysis Date = 01/22/15 
 Pct Recovery = 98%  Analysis Date = 01/22/15 
 Pct Recovery = 98%  Analysis Date = 01/18/15 
 Pct Recovery = 98%  Analysis Date = 01/18/15 
 Pct Recovery = 98%  Analysis Date = 01/14/15 
 Pct Recovery = 98%  Analysis Date = 01/14/15 
 Pct Recovery = 98%  Analysis Date = 01/10/15 
 Pct Recovery = 98%  Analysis Date = 01/10/15 
 Pct Recovery = 98%  Analysis Date = 01/06/15 
 Pct Recovery = 98%  Analysis Date = 01/06/15 
 Pct Recovery = 98%  Analysis Date = 01/02/15 
 Pct Recovery = 99%  Analysis Date = 01/02/15 
 Pct Recovery = 99%  Analysis Date = 12/28/14 
 Pct Recovery = 99%  Analysis Date = 12/28/14 
 Pct Recovery = 99%  Analysis Date = 12/24/14 
 Pct Recovery = 99%  Analysis Date = 12/24/14 
 Pct Recovery = 99%  Analysis Date = 12/20/14 
 Pct Recovery = 99%  Analysis Date = 12/20/14 
 Pct Recovery = 99%  Analysis Date = 12/16/14 
 Pct Recovery = 99%  Analysis Date = 12/16/14 
 Pct Recovery = 99%  Analysis Date = 12/12/14 
 Pct Recovery = 99%  Analysis Date = 12/12/14 
 Pct Recovery = 99%  Analysis Date = 12/08/14 
 Pct Recovery = 99%  Analysis Date = 12/08/14 
 Pct Recovery = 99%  Analysis Date = 12/04/14 
 Pct Recovery = 99%  Analysis Date = 12/04/14 
 Pct Recovery = 99%  Analysis Date = 11/29/14 
 Pct Recovery = 100%  Analysis Date = 11/29/14 
 Pct Recovery = 100%  Analysis Date = 11/25/14 
 Pct Recovery = 100%  Analysis Date = 11/25/14 
 Pct Recovery = 100%  Analysis Date = 11/21/14 
 Pct Recovery = 100%  Analysis Date = 11/21/14 
 Pct Recovery = 100%  Analysis Date = 11/17/14 
 Pct Recovery = 100%  Analysis Date = 11/17/14 
 Pct Recovery = 100%  Analysis Date = 11/13/14 
 Pct Recovery = 100%  Analysis Date = 11/13/14 
 Pct Recovery = 100%  Analysis Date = 11/09/14 
 Pct Recovery = 101%  Analysis Date = 11/09/14 
 Pct Recovery = 101%  Analysis Date = 11/05/14 
 Pct Recovery = 101%  Analysis Date = 11/05/14 
 Pct Recovery = 101%  Analysis Date = 11/01/14 
 Pct Recovery = 101%  Analysis Date = 11/01/14 
 Pct Recovery = 101%  Analysis Date = 10/27/14 
 Pct Recovery = 101%  Analysis Date = 10/27/14 
 Pct Recovery = 101%  Analysis Date = 10/23/14 
 Pct Recovery = 101%  Analysis Date = 10/23/14 
 Pct Recovery = 101%  Analysis Date = 10/19/14 
 Pct Recovery = 102%  Analysis Date = 10/19/14 
 Pct Recovery = 102%  Analysis Date = 10/15/14 
 Pct Recovery = 102%  Analysis Date = 10/15/14 
 Pct Recovery = 102%  Analysis Date = 10/11/14 
 Pct Recovery = 102%  Analysis Date = 10/11/14 
 Pct Recovery = 102%  Analysis Date = 10/07/14 
 Pct Recovery = 102%  Analysis Date = 10/07/14 
 Pct Recovery = 102%  Analysis Date = 10/03/14 
 Pct Recovery = 103%  Analysis Date = 10/03/14 
 Pct Recovery = 103%  Analysis Date = 09/28/14 
 Pct Recovery = 103%  Analysis Date = 09/28/14 
 Pct Recovery = 103%  Analysis Date = 09/24/14 
 Pct Recovery = 103%  Analysis Date = 09/24/14 
 Pct Recovery = 103%  Analysis Date = 09/20/14 
 Pct Recovery = 103%  Analysis Date = 09/20/14 
 Pct Recovery = 103%  Analysis Date = 09/16/14 
 Pct Recovery = 103%  Analysis Date = 09/16/14 
 Pct Recovery = 103%  Analysis Date = 09/12/14 
 Pct Recovery = 104%  Analysis Date = 09/12/14 
 Pct Recovery = 104%  Analysis Date = 09/08/14 
 Pct Recovery = 104%  Analysis Date = 09/08/14 
 Pct Recovery = 104%  Analysis Date = 09/04/14 
 Pct Recovery = 104%  Analysis Date = 09/04/14 
 Pct Recovery = 104%  Analysis Date = 08/30/14 
 Pct Recovery = 104%  Analysis Date = 08/30/14 
 Pct Recovery = 104%  Analysis Date = 08/26/14 
 Pct Recovery = 104%  Analysis Date = 08/26/14 
 Pct Recovery = 104%  Analysis Date = 08/22/14 
 Pct Recovery = 105%  Analysis Date = 08/22/14 
 Pct Recovery = 105%  Analysis Date = 08/18/14 
 Pct Recovery = 105%  Analysis Date = 08/18/14 
 Pct Recovery = 105%  Analysis Date = 08/14/14 
 Pct Recovery = 105%  Analysis Date = 08/14/14 
 Pct Recovery = 105%  Analysis Date = 08/10/14 
 Pct Recovery = 105%  Analysis Date = 08/10/14 
 Pct Recovery = 105%  Analysis Date = 08/06/14 
 Pct Recovery = 106%  Analysis Date = 08/06/14 
 Pct Recovery = 106%  Analysis Date = 08/01/14 
 Pct Recovery = 106%  Analysis Date = 08/01/14 
 Pct Recovery = 106%  Analysis Date = 07/28/14 
 Pct Recovery = 106%  Analysis Date = 07/28/14 
 Pct Recovery = 106%  Analysis Date = 07/24/14 
 Pct Recovery = 106%  Analysis Date = 07/24/14 
 Pct Recovery = 106%  Analysis Date = 07/20/14 
 Pct Recovery = 106%  Analysis Date = 07/20/14 
 Pct Recovery = 106%  Analysis Date = 07/16/14 
 Pct Recovery = 107%  Analysis Date = 07/16/14 
 Pct Recovery = 107%  Analysis Date = 07/12/14 
 Pct Recovery = 107%  Analysis Date = 07/12/14 
 Pct Recovery = 107%  Analysis Date = 07/08/14 
 Pct Recovery = 107%  Analysis Date = 07/08/14 
 Pct Recovery = 107%  Analysis Date = 07/03/14 
 Pct Recovery = 107%  Analysis Date = 07/03/14 
 Pct Recovery = 107%  Analysis Date = 06/29/14 
 Pct Recovery = 108%  Analysis Date = 06/29/14 
 Pct Recovery = 108%  Analysis Date = 06/25/14 
 Pct Recovery = 108%  Analysis Date = 06/25/14 
 Pct Recovery = 108%  Analysis Date = 06/21/14 
 Pct Recovery = 108%  Analysis Date = 06/21/14 
 Pct Recovery = 108%  Analysis Date = 06/17/14 
 Pct Recovery = 108%  Analysis Date = 06/17/14 
 Pct Recovery = 108%  Analysis Date = 06/13/14 
 Pct Recovery = 109%  Analysis Date = 06/13/14 
 Pct Recovery = 109%  Analysis Date = 06/09/14 
 Pct Recovery = 109%  Analysis Date = 06/09/14 
 Pct Recovery = 109%  Analysis Date = 06/04/14 
 Pct Recovery = 109%  Analysis Date = 06/04/14 
 Pct Recovery = 109%  Analysis Date = 05/31/14 
 Pct Recovery = 109%  Analysis Date = 05/31/14 
 Pct Recovery = 109%  Analysis Date = 05/27/14 
 Pct Recovery = 109%  Analysis Date = 05/27/14 
 Pct Recovery = 109%  Analysis Date = 05/23/14 
 Pct Recovery = 110%  Analysis Date = 05/23/14 
 Pct Recovery = 110%  Analysis Date = 05/19/14 
 Pct Recovery = 110%  Analysis Date = 05/19/14 
 Pct Recovery = 110%  Analysis Date = 05/15/14 
 Pct Recovery = 110%  Analysis Date = 05/15/14 
 Pct Recovery = 110%  Analysis Date = 05/11/14 
 Pct Recovery = 110%  Analysis Date = 05/11/14 
 Pct Recovery = 110%  Analysis Date = 05/07/14 
 Pct Recovery = 111%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
HEXANOL, 2-ETHYL-

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 46 97% 16% 96% 12%
Total 46 97% 16% 96% 12%

Sample Statistics
HEXANOL, 2-ETHYL-

Characteristic N % % Basis
Plotted 46 100% Spiked
Estimated Values 40 87% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 46 .  
False Negatives 0 0% 0 out of 46
Not Spiked 27 .  
False Positives 0 0% 0 out of 27

BQS OBSP Determination:
ISOPHORONE
METHOD: 4437 , TESTIDCODE: 34408GM016
Open Data Set

 Analysis Date = 07/29/16 
 SpikeMix = Supelco LC20145V: 40 µl & NSI 041516: 40 µl & NSI 041416HVOC: 40 µl 
 Pct Recovery = 75%  Analysis Date = 07/06/16 
 SpikeMix = Accu 216041354: 40 µl & NSI 041516: 40 µl & NSI 041416HVOC: 40 µl 
 Pct Recovery = 88%  Analysis Date = 08/11/16 
 SpikeMix = Phenova B20160303: 25 µl & Supelco LC20145V: 25 µl & NSI 041416HVOC: 25 µl 
 Pct Recovery = 76%  Analysis Date = 05/21/16 
 SpikeMix = Supelco LC20145V: 25 µl & NSI 041516: 25 µl & NSI 041416HVOC: 25 µl 
 Pct Recovery = 101%  Analysis Date = 03/19/15 
 SpikeMix = Supelco LC06437: 20 µl & NSI 031814: 20 µl 
 Pct Recovery = 121%  Analysis Date = 06/06/14 
 SpikeMix = NSI 031814: 20 µl & ChemService 2615700: 20 µl 
 Pct Recovery = 125%  Analysis Date = 05/07/14 
 SpikeMix = NSI 031814: 20 µl & Accu 214031128: 20 µl 
 Pct Recovery = 124%  Analysis Date = 01/10/15 
 SpikeMix = Abs 032014: 20 µl & ERA 0321-14-05A: 20 µl 
 Pct Recovery = 100%  Analysis Date = 08/20/14 
 SpikeMix = Supelco LC06437: 20 µl & Abs 032014: 20 µl 
 Pct Recovery = 120%  Analysis Date = 07/23/14 
 SpikeMix = Accu 214031128: 20 µl & Abs 032014: 20 µl 
 Pct Recovery = 113%  Analysis Date = 07/03/14 
 SpikeMix = Abs 032014: 20 µl & ChemService 2615700: 20 µl 
 Pct Recovery = 123%  Analysis Date = 06/26/15 
 SpikeMix = ChemService 3818700: 25 µl & Accu 215041338: 25 µl 
 Pct Recovery = 85%  Analysis Date = 06/25/15 
 SpikeMix = ChemService 3818700: 25 µl & NSI 050515HVOC: 25 µl 
 Pct Recovery = 85%  Analysis Date = 01/22/16 
 SpikeMix = NSI 050515HVOC: 25 µl & ERA 0601-15-05: 25 µl 
 Pct Recovery = 74%  Analysis Date = 10/09/15 
 SpikeMix = ERA 0601-15-05: 25 µl & Accu 215041338: 25 µl 
 Pct Recovery = 83%  Analysis Date = 07/27/16 
 SpikeMix = ChemService 5082800: 15 µl & Supelco LC20145V: 15 µl & Accu 216041225: 15 µl 
 Pct Recovery = 71%  Analysis Date = 08/12/16 
 SpikeMix = Accu 216041354: 15 µl & Abs 060916HVOC: 15 µl 
 Pct Recovery = 77%  Analysis Date = 07/06/16 
 SpikeMix = Phenova B20160303: 15 µl & Accu 216041354: 15 µl & NSI 041416HVOC: 15 µl 
 Pct Recovery = 73%  Analysis Date = 06/23/16 
 SpikeMix = . 
 Pct Recovery = 38%  Analysis Date = 05/20/16 
 SpikeMix = Accu 216041354: 15 µl & NSI 041516: 15 µl & Accu 216041225: 15 µl 
 Pct Recovery = 83%  Analysis Date = 04/28/16 
 SpikeMix = ChemService 3818700: 15 µl & Supelco LC13544: 15 µl 
 Pct Recovery = 104%  Analysis Date = 06/16/15 
 SpikeMix = ChemService 3818700: 15 µl & NSI 050515HVOC: 15 µl 
 Pct Recovery = 83%  Analysis Date = 05/14/15 
 SpikeMix = ChemService 3818700: 15 µl & Supelco LC13544: 15 µl 
 Pct Recovery = 102%  Analysis Date = 09/24/15 
 SpikeMix = Abs 040315: 15 µl & ERA 0601-15-05: 15 µl 
 Pct Recovery = 76%  Analysis Date = 08/24/15 
 SpikeMix = ERA 0601-15-05: 15 µl & Supelco LC13544: 15 µl 
 Pct Recovery = 84%  Analysis Date = 12/13/14 
 SpikeMix = Accu 214031128: 10 µl & NSI 031814: 10 µl 
 Pct Recovery = 122%  Analysis Date = 07/30/14 
 SpikeMix = NSI 031814: 10 µl & ChemService 2615700: 10 µl 
 Pct Recovery = 156%  Analysis Date = 04/25/15 
 SpikeMix = Abs 032014: 10 µl & ERA 0321-14-05A: 10 µl 
 Pct Recovery = 97%  Analysis Date = 09/11/14 
 SpikeMix = Accu 214031128: 10 µl & Abs 032014: 10 µl 
 Pct Recovery = 71%  Analysis Date = 06/17/14 
 SpikeMix = Supelco LC06437: 10 µl & Abs 032014: 10 µl 
 Pct Recovery = 118%  Analysis Date = 04/09/16 
 SpikeMix = Abs 040315: 10 µl & ChemService 3818700: 10 µl 
 Pct Recovery = 85%  Analysis Date = 12/10/15 
 SpikeMix = ChemService 3818700: 10 µl & Supelco LC13544: 10 µl 
 Pct Recovery = 84%  Analysis Date = 10/23/15 
 SpikeMix = Abs 040315: 10 µl & ChemService 3818700: 10 µl 
 Pct Recovery = 100%  Analysis Date = 05/20/15 
 SpikeMix = ChemService 3818700: 10 µl & Accu 215041338: 10 µl 
 Pct Recovery = 110%  Analysis Date = 02/12/16 
 SpikeMix = ERA 0601-15-05: 10 µl & Accu 215041338: 10 µl 
 Pct Recovery = 77%  Analysis Date = 12/05/15 
 SpikeMix = NSI 050515HVOC: 10 µl & ERA 0601-15-05: 10 µl 
 Pct Recovery = 72%  Analysis Date = 11/14/15 
 SpikeMix = ERA 0601-15-05: 10 µl 
 Pct Recovery = 69%  Analysis Date = 08/14/15 
 SpikeMix = Abs 040315: 10 µl & ERA 0601-15-05: 10 µl 
 Pct Recovery = 59%  Analysis Date = 08/11/16 
 Pct Recovery = 76%  Analysis Date = 08/07/16 
 Pct Recovery = 76%  Analysis Date = 08/07/16 
 Pct Recovery = 76%  Analysis Date = 08/03/16 
 Pct Recovery = 77%  Analysis Date = 08/03/16 
 Pct Recovery = 77%  Analysis Date = 07/30/16 
 Pct Recovery = 77%  Analysis Date = 07/30/16 
 Pct Recovery = 77%  Analysis Date = 07/26/16 
 Pct Recovery = 77%  Analysis Date = 07/26/16 
 Pct Recovery = 77%  Analysis Date = 07/22/16 
 Pct Recovery = 77%  Analysis Date = 07/22/16 
 Pct Recovery = 77%  Analysis Date = 07/18/16 
 Pct Recovery = 77%  Analysis Date = 07/18/16 
 Pct Recovery = 77%  Analysis Date = 07/14/16 
 Pct Recovery = 77%  Analysis Date = 07/14/16 
 Pct Recovery = 77%  Analysis Date = 07/09/16 
 Pct Recovery = 77%  Analysis Date = 07/09/16 
 Pct Recovery = 77%  Analysis Date = 07/05/16 
 Pct Recovery = 77%  Analysis Date = 07/05/16 
 Pct Recovery = 77%  Analysis Date = 07/01/16 
 Pct Recovery = 77%  Analysis Date = 07/01/16 
 Pct Recovery = 77%  Analysis Date = 06/27/16 
 Pct Recovery = 78%  Analysis Date = 06/27/16 
 Pct Recovery = 78%  Analysis Date = 06/23/16 
 Pct Recovery = 78%  Analysis Date = 06/23/16 
 Pct Recovery = 78%  Analysis Date = 06/19/16 
 Pct Recovery = 78%  Analysis Date = 06/19/16 
 Pct Recovery = 78%  Analysis Date = 06/15/16 
 Pct Recovery = 78%  Analysis Date = 06/15/16 
 Pct Recovery = 78%  Analysis Date = 06/10/16 
 Pct Recovery = 78%  Analysis Date = 06/10/16 
 Pct Recovery = 78%  Analysis Date = 06/06/16 
 Pct Recovery = 78%  Analysis Date = 06/06/16 
 Pct Recovery = 78%  Analysis Date = 06/02/16 
 Pct Recovery = 78%  Analysis Date = 06/02/16 
 Pct Recovery = 78%  Analysis Date = 05/29/16 
 Pct Recovery = 78%  Analysis Date = 05/29/16 
 Pct Recovery = 78%  Analysis Date = 05/25/16 
 Pct Recovery = 78%  Analysis Date = 05/25/16 
 Pct Recovery = 78%  Analysis Date = 05/21/16 
 Pct Recovery = 78%  Analysis Date = 05/21/16 
 Pct Recovery = 78%  Analysis Date = 05/17/16 
 Pct Recovery = 78%  Analysis Date = 05/17/16 
 Pct Recovery = 78%  Analysis Date = 05/12/16 
 Pct Recovery = 78%  Analysis Date = 05/12/16 
 Pct Recovery = 78%  Analysis Date = 05/08/16 
 Pct Recovery = 79%  Analysis Date = 05/08/16 
 Pct Recovery = 79%  Analysis Date = 05/04/16 
 Pct Recovery = 79%  Analysis Date = 05/04/16 
 Pct Recovery = 79%  Analysis Date = 04/30/16 
 Pct Recovery = 79%  Analysis Date = 04/30/16 
 Pct Recovery = 79%  Analysis Date = 04/26/16 
 Pct Recovery = 79%  Analysis Date = 04/26/16 
 Pct Recovery = 79%  Analysis Date = 04/22/16 
 Pct Recovery = 79%  Analysis Date = 04/22/16 
 Pct Recovery = 79%  Analysis Date = 04/18/16 
 Pct Recovery = 79%  Analysis Date = 04/18/16 
 Pct Recovery = 79%  Analysis Date = 04/13/16 
 Pct Recovery = 79%  Analysis Date = 04/13/16 
 Pct Recovery = 79%  Analysis Date = 04/09/16 
 Pct Recovery = 79%  Analysis Date = 04/09/16 
 Pct Recovery = 79%  Analysis Date = 04/05/16 
 Pct Recovery = 79%  Analysis Date = 04/05/16 
 Pct Recovery = 79%  Analysis Date = 04/01/16 
 Pct Recovery = 79%  Analysis Date = 04/01/16 
 Pct Recovery = 79%  Analysis Date = 03/28/16 
 Pct Recovery = 80%  Analysis Date = 03/28/16 
 Pct Recovery = 80%  Analysis Date = 03/24/16 
 Pct Recovery = 80%  Analysis Date = 03/24/16 
 Pct Recovery = 80%  Analysis Date = 03/20/16 
 Pct Recovery = 80%  Analysis Date = 03/20/16 
 Pct Recovery = 80%  Analysis Date = 03/15/16 
 Pct Recovery = 80%  Analysis Date = 03/15/16 
 Pct Recovery = 80%  Analysis Date = 03/11/16 
 Pct Recovery = 80%  Analysis Date = 03/11/16 
 Pct Recovery = 80%  Analysis Date = 03/07/16 
 Pct Recovery = 80%  Analysis Date = 03/07/16 
 Pct Recovery = 80%  Analysis Date = 03/03/16 
 Pct Recovery = 80%  Analysis Date = 03/03/16 
 Pct Recovery = 80%  Analysis Date = 02/28/16 
 Pct Recovery = 80%  Analysis Date = 02/28/16 
 Pct Recovery = 80%  Analysis Date = 02/24/16 
 Pct Recovery = 80%  Analysis Date = 02/24/16 
 Pct Recovery = 80%  Analysis Date = 02/20/16 
 Pct Recovery = 80%  Analysis Date = 02/20/16 
 Pct Recovery = 80%  Analysis Date = 02/15/16 
 Pct Recovery = 81%  Analysis Date = 02/15/16 
 Pct Recovery = 81%  Analysis Date = 02/11/16 
 Pct Recovery = 81%  Analysis Date = 02/11/16 
 Pct Recovery = 81%  Analysis Date = 02/07/16 
 Pct Recovery = 81%  Analysis Date = 02/07/16 
 Pct Recovery = 81%  Analysis Date = 02/03/16 
 Pct Recovery = 81%  Analysis Date = 02/03/16 
 Pct Recovery = 81%  Analysis Date = 01/30/16 
 Pct Recovery = 81%  Analysis Date = 01/30/16 
 Pct Recovery = 81%  Analysis Date = 01/26/16 
 Pct Recovery = 81%  Analysis Date = 01/26/16 
 Pct Recovery = 81%  Analysis Date = 01/22/16 
 Pct Recovery = 81%  Analysis Date = 01/22/16 
 Pct Recovery = 81%  Analysis Date = 01/17/16 
 Pct Recovery = 81%  Analysis Date = 01/17/16 
 Pct Recovery = 81%  Analysis Date = 01/13/16 
 Pct Recovery = 80%  Analysis Date = 01/13/16 
 Pct Recovery = 80%  Analysis Date = 01/09/16 
 Pct Recovery = 80%  Analysis Date = 01/09/16 
 Pct Recovery = 80%  Analysis Date = 01/05/16 
 Pct Recovery = 80%  Analysis Date = 01/05/16 
 Pct Recovery = 80%  Analysis Date = 01/01/16 
 Pct Recovery = 80%  Analysis Date = 01/01/16 
 Pct Recovery = 80%  Analysis Date = 12/28/15 
 Pct Recovery = 80%  Analysis Date = 12/28/15 
 Pct Recovery = 80%  Analysis Date = 12/24/15 
 Pct Recovery = 80%  Analysis Date = 12/24/15 
 Pct Recovery = 80%  Analysis Date = 12/20/15 
 Pct Recovery = 80%  Analysis Date = 12/20/15 
 Pct Recovery = 80%  Analysis Date = 12/15/15 
 Pct Recovery = 80%  Analysis Date = 12/15/15 
 Pct Recovery = 80%  Analysis Date = 12/11/15 
 Pct Recovery = 80%  Analysis Date = 12/11/15 
 Pct Recovery = 80%  Analysis Date = 12/07/15 
 Pct Recovery = 80%  Analysis Date = 12/07/15 
 Pct Recovery = 80%  Analysis Date = 12/03/15 
 Pct Recovery = 80%  Analysis Date = 12/03/15 
 Pct Recovery = 80%  Analysis Date = 11/29/15 
 Pct Recovery = 80%  Analysis Date = 11/29/15 
 Pct Recovery = 80%  Analysis Date = 11/25/15 
 Pct Recovery = 80%  Analysis Date = 11/25/15 
 Pct Recovery = 80%  Analysis Date = 11/21/15 
 Pct Recovery = 81%  Analysis Date = 11/21/15 
 Pct Recovery = 81%  Analysis Date = 11/16/15 
 Pct Recovery = 81%  Analysis Date = 11/16/15 
 Pct Recovery = 81%  Analysis Date = 11/12/15 
 Pct Recovery = 81%  Analysis Date = 11/12/15 
 Pct Recovery = 81%  Analysis Date = 11/08/15 
 Pct Recovery = 81%  Analysis Date = 11/08/15 
 Pct Recovery = 81%  Analysis Date = 11/04/15 
 Pct Recovery = 81%  Analysis Date = 11/04/15 
 Pct Recovery = 81%  Analysis Date = 10/31/15 
 Pct Recovery = 81%  Analysis Date = 10/31/15 
 Pct Recovery = 81%  Analysis Date = 10/27/15 
 Pct Recovery = 81%  Analysis Date = 10/27/15 
 Pct Recovery = 81%  Analysis Date = 10/23/15 
 Pct Recovery = 81%  Analysis Date = 10/23/15 
 Pct Recovery = 81%  Analysis Date = 10/18/15 
 Pct Recovery = 81%  Analysis Date = 10/18/15 
 Pct Recovery = 81%  Analysis Date = 10/14/15 
 Pct Recovery = 82%  Analysis Date = 10/14/15 
 Pct Recovery = 82%  Analysis Date = 10/10/15 
 Pct Recovery = 82%  Analysis Date = 10/10/15 
 Pct Recovery = 82%  Analysis Date = 10/06/15 
 Pct Recovery = 82%  Analysis Date = 10/06/15 
 Pct Recovery = 82%  Analysis Date = 10/02/15 
 Pct Recovery = 82%  Analysis Date = 10/02/15 
 Pct Recovery = 82%  Analysis Date = 09/28/15 
 Pct Recovery = 83%  Analysis Date = 09/28/15 
 Pct Recovery = 83%  Analysis Date = 09/24/15 
 Pct Recovery = 83%  Analysis Date = 09/24/15 
 Pct Recovery = 83%  Analysis Date = 09/19/15 
 Pct Recovery = 83%  Analysis Date = 09/19/15 
 Pct Recovery = 83%  Analysis Date = 09/15/15 
 Pct Recovery = 84%  Analysis Date = 09/15/15 
 Pct Recovery = 84%  Analysis Date = 09/11/15 
 Pct Recovery = 84%  Analysis Date = 09/11/15 
 Pct Recovery = 84%  Analysis Date = 09/07/15 
 Pct Recovery = 84%  Analysis Date = 09/07/15 
 Pct Recovery = 84%  Analysis Date = 09/03/15 
 Pct Recovery = 85%  Analysis Date = 09/03/15 
 Pct Recovery = 85%  Analysis Date = 08/30/15 
 Pct Recovery = 85%  Analysis Date = 08/30/15 
 Pct Recovery = 85%  Analysis Date = 08/26/15 
 Pct Recovery = 85%  Analysis Date = 08/26/15 
 Pct Recovery = 85%  Analysis Date = 08/21/15 
 Pct Recovery = 86%  Analysis Date = 08/21/15 
 Pct Recovery = 86%  Analysis Date = 08/17/15 
 Pct Recovery = 86%  Analysis Date = 08/17/15 
 Pct Recovery = 86%  Analysis Date = 08/13/15 
 Pct Recovery = 86%  Analysis Date = 08/13/15 
 Pct Recovery = 86%  Analysis Date = 08/09/15 
 Pct Recovery = 87%  Analysis Date = 08/09/15 
 Pct Recovery = 87%  Analysis Date = 08/05/15 
 Pct Recovery = 87%  Analysis Date = 08/05/15 
 Pct Recovery = 87%  Analysis Date = 08/01/15 
 Pct Recovery = 88%  Analysis Date = 08/01/15 
 Pct Recovery = 88%  Analysis Date = 07/28/15 
 Pct Recovery = 88%  Analysis Date = 07/28/15 
 Pct Recovery = 88%  Analysis Date = 07/23/15 
 Pct Recovery = 89%  Analysis Date = 07/23/15 
 Pct Recovery = 89%  Analysis Date = 07/19/15 
 Pct Recovery = 89%  Analysis Date = 07/19/15 
 Pct Recovery = 89%  Analysis Date = 07/15/15 
 Pct Recovery = 90%  Analysis Date = 07/15/15 
 Pct Recovery = 90%  Analysis Date = 07/11/15 
 Pct Recovery = 90%  Analysis Date = 07/11/15 
 Pct Recovery = 90%  Analysis Date = 07/07/15 
 Pct Recovery = 90%  Analysis Date = 07/07/15 
 Pct Recovery = 90%  Analysis Date = 07/03/15 
 Pct Recovery = 91%  Analysis Date = 07/03/15 
 Pct Recovery = 91%  Analysis Date = 06/29/15 
 Pct Recovery = 91%  Analysis Date = 06/29/15 
 Pct Recovery = 91%  Analysis Date = 06/24/15 
 Pct Recovery = 92%  Analysis Date = 06/24/15 
 Pct Recovery = 92%  Analysis Date = 06/20/15 
 Pct Recovery = 92%  Analysis Date = 06/20/15 
 Pct Recovery = 92%  Analysis Date = 06/16/15 
 Pct Recovery = 93%  Analysis Date = 06/16/15 
 Pct Recovery = 93%  Analysis Date = 06/12/15 
 Pct Recovery = 93%  Analysis Date = 06/12/15 
 Pct Recovery = 93%  Analysis Date = 06/08/15 
 Pct Recovery = 94%  Analysis Date = 06/08/15 
 Pct Recovery = 94%  Analysis Date = 06/04/15 
 Pct Recovery = 94%  Analysis Date = 06/04/15 
 Pct Recovery = 94%  Analysis Date = 05/31/15 
 Pct Recovery = 94%  Analysis Date = 05/31/15 
 Pct Recovery = 94%  Analysis Date = 05/27/15 
 Pct Recovery = 95%  Analysis Date = 05/27/15 
 Pct Recovery = 95%  Analysis Date = 05/22/15 
 Pct Recovery = 95%  Analysis Date = 05/22/15 
 Pct Recovery = 95%  Analysis Date = 05/18/15 
 Pct Recovery = 96%  Analysis Date = 05/18/15 
 Pct Recovery = 96%  Analysis Date = 05/14/15 
 Pct Recovery = 96%  Analysis Date = 05/14/15 
 Pct Recovery = 96%  Analysis Date = 05/10/15 
 Pct Recovery = 97%  Analysis Date = 05/10/15 
 Pct Recovery = 97%  Analysis Date = 05/06/15 
 Pct Recovery = 97%  Analysis Date = 05/06/15 
 Pct Recovery = 97%  Analysis Date = 05/02/15 
 Pct Recovery = 97%  Analysis Date = 05/02/15 
 Pct Recovery = 97%  Analysis Date = 04/28/15 
 Pct Recovery = 98%  Analysis Date = 04/28/15 
 Pct Recovery = 98%  Analysis Date = 04/23/15 
 Pct Recovery = 98%  Analysis Date = 04/23/15 
 Pct Recovery = 98%  Analysis Date = 04/19/15 
 Pct Recovery = 98%  Analysis Date = 04/19/15 
 Pct Recovery = 98%  Analysis Date = 04/15/15 
 Pct Recovery = 99%  Analysis Date = 04/15/15 
 Pct Recovery = 99%  Analysis Date = 04/11/15 
 Pct Recovery = 99%  Analysis Date = 04/11/15 
 Pct Recovery = 99%  Analysis Date = 04/07/15 
 Pct Recovery = 99%  Analysis Date = 04/07/15 
 Pct Recovery = 99%  Analysis Date = 04/03/15 
 Pct Recovery = 100%  Analysis Date = 04/03/15 
 Pct Recovery = 100%  Analysis Date = 03/30/15 
 Pct Recovery = 100%  Analysis Date = 03/30/15 
 Pct Recovery = 100%  Analysis Date = 03/25/15 
 Pct Recovery = 100%  Analysis Date = 03/25/15 
 Pct Recovery = 100%  Analysis Date = 03/21/15 
 Pct Recovery = 101%  Analysis Date = 03/21/15 
 Pct Recovery = 101%  Analysis Date = 03/17/15 
 Pct Recovery = 101%  Analysis Date = 03/17/15 
 Pct Recovery = 101%  Analysis Date = 03/13/15 
 Pct Recovery = 101%  Analysis Date = 03/13/15 
 Pct Recovery = 101%  Analysis Date = 03/09/15 
 Pct Recovery = 102%  Analysis Date = 03/09/15 
 Pct Recovery = 102%  Analysis Date = 03/05/15 
 Pct Recovery = 102%  Analysis Date = 03/05/15 
 Pct Recovery = 102%  Analysis Date = 03/01/15 
 Pct Recovery = 102%  Analysis Date = 03/01/15 
 Pct Recovery = 102%  Analysis Date = 02/24/15 
 Pct Recovery = 103%  Analysis Date = 02/24/15 
 Pct Recovery = 103%  Analysis Date = 02/20/15 
 Pct Recovery = 103%  Analysis Date = 02/20/15 
 Pct Recovery = 103%  Analysis Date = 02/16/15 
 Pct Recovery = 103%  Analysis Date = 02/16/15 
 Pct Recovery = 103%  Analysis Date = 02/12/15 
 Pct Recovery = 104%  Analysis Date = 02/12/15 
 Pct Recovery = 104%  Analysis Date = 02/08/15 
 Pct Recovery = 104%  Analysis Date = 02/08/15 
 Pct Recovery = 104%  Analysis Date = 02/04/15 
 Pct Recovery = 104%  Analysis Date = 02/04/15 
 Pct Recovery = 104%  Analysis Date = 01/31/15 
 Pct Recovery = 105%  Analysis Date = 01/31/15 
 Pct Recovery = 105%  Analysis Date = 01/26/15 
 Pct Recovery = 105%  Analysis Date = 01/26/15 
 Pct Recovery = 105%  Analysis Date = 01/22/15 
 Pct Recovery = 105%  Analysis Date = 01/22/15 
 Pct Recovery = 105%  Analysis Date = 01/18/15 
 Pct Recovery = 106%  Analysis Date = 01/18/15 
 Pct Recovery = 106%  Analysis Date = 01/14/15 
 Pct Recovery = 106%  Analysis Date = 01/14/15 
 Pct Recovery = 106%  Analysis Date = 01/10/15 
 Pct Recovery = 106%  Analysis Date = 01/10/15 
 Pct Recovery = 106%  Analysis Date = 01/06/15 
 Pct Recovery = 107%  Analysis Date = 01/06/15 
 Pct Recovery = 107%  Analysis Date = 01/02/15 
 Pct Recovery = 107%  Analysis Date = 01/02/15 
 Pct Recovery = 107%  Analysis Date = 12/28/14 
 Pct Recovery = 107%  Analysis Date = 12/28/14 
 Pct Recovery = 107%  Analysis Date = 12/24/14 
 Pct Recovery = 108%  Analysis Date = 12/24/14 
 Pct Recovery = 108%  Analysis Date = 12/20/14 
 Pct Recovery = 108%  Analysis Date = 12/20/14 
 Pct Recovery = 108%  Analysis Date = 12/16/14 
 Pct Recovery = 108%  Analysis Date = 12/16/14 
 Pct Recovery = 108%  Analysis Date = 12/12/14 
 Pct Recovery = 109%  Analysis Date = 12/12/14 
 Pct Recovery = 109%  Analysis Date = 12/08/14 
 Pct Recovery = 109%  Analysis Date = 12/08/14 
 Pct Recovery = 109%  Analysis Date = 12/04/14 
 Pct Recovery = 109%  Analysis Date = 12/04/14 
 Pct Recovery = 109%  Analysis Date = 11/29/14 
 Pct Recovery = 110%  Analysis Date = 11/29/14 
 Pct Recovery = 110%  Analysis Date = 11/25/14 
 Pct Recovery = 110%  Analysis Date = 11/25/14 
 Pct Recovery = 110%  Analysis Date = 11/21/14 
 Pct Recovery = 110%  Analysis Date = 11/21/14 
 Pct Recovery = 110%  Analysis Date = 11/17/14 
 Pct Recovery = 111%  Analysis Date = 11/17/14 
 Pct Recovery = 111%  Analysis Date = 11/13/14 
 Pct Recovery = 111%  Analysis Date = 11/13/14 
 Pct Recovery = 111%  Analysis Date = 11/09/14 
 Pct Recovery = 111%  Analysis Date = 11/09/14 
 Pct Recovery = 111%  Analysis Date = 11/05/14 
 Pct Recovery = 112%  Analysis Date = 11/05/14 
 Pct Recovery = 112%  Analysis Date = 11/01/14 
 Pct Recovery = 112%  Analysis Date = 11/01/14 
 Pct Recovery = 112%  Analysis Date = 10/27/14 
 Pct Recovery = 112%  Analysis Date = 10/27/14 
 Pct Recovery = 112%  Analysis Date = 10/23/14 
 Pct Recovery = 113%  Analysis Date = 10/23/14 
 Pct Recovery = 113%  Analysis Date = 10/19/14 
 Pct Recovery = 113%  Analysis Date = 10/19/14 
 Pct Recovery = 113%  Analysis Date = 10/15/14 
 Pct Recovery = 113%  Analysis Date = 10/15/14 
 Pct Recovery = 113%  Analysis Date = 10/11/14 
 Pct Recovery = 114%  Analysis Date = 10/11/14 
 Pct Recovery = 114%  Analysis Date = 10/07/14 
 Pct Recovery = 114%  Analysis Date = 10/07/14 
 Pct Recovery = 114%  Analysis Date = 10/03/14 
 Pct Recovery = 114%  Analysis Date = 10/03/14 
 Pct Recovery = 114%  Analysis Date = 09/28/14 
 Pct Recovery = 115%  Analysis Date = 09/28/14 
 Pct Recovery = 115%  Analysis Date = 09/24/14 
 Pct Recovery = 115%  Analysis Date = 09/24/14 
 Pct Recovery = 115%  Analysis Date = 09/20/14 
 Pct Recovery = 115%  Analysis Date = 09/20/14 
 Pct Recovery = 115%  Analysis Date = 09/16/14 
 Pct Recovery = 116%  Analysis Date = 09/16/14 
 Pct Recovery = 116%  Analysis Date = 09/12/14 
 Pct Recovery = 116%  Analysis Date = 09/12/14 
 Pct Recovery = 116%  Analysis Date = 09/08/14 
 Pct Recovery = 116%  Analysis Date = 09/08/14 
 Pct Recovery = 116%  Analysis Date = 09/04/14 
 Pct Recovery = 116%  Analysis Date = 09/04/14 
 Pct Recovery = 116%  Analysis Date = 08/30/14 
 Pct Recovery = 117%  Analysis Date = 08/30/14 
 Pct Recovery = 117%  Analysis Date = 08/26/14 
 Pct Recovery = 117%  Analysis Date = 08/26/14 
 Pct Recovery = 117%  Analysis Date = 08/22/14 
 Pct Recovery = 117%  Analysis Date = 08/22/14 
 Pct Recovery = 117%  Analysis Date = 08/18/14 
 Pct Recovery = 118%  Analysis Date = 08/18/14 
 Pct Recovery = 118%  Analysis Date = 08/14/14 
 Pct Recovery = 118%  Analysis Date = 08/14/14 
 Pct Recovery = 118%  Analysis Date = 08/10/14 
 Pct Recovery = 118%  Analysis Date = 08/10/14 
 Pct Recovery = 118%  Analysis Date = 08/06/14 
 Pct Recovery = 119%  Analysis Date = 08/06/14 
 Pct Recovery = 119%  Analysis Date = 08/01/14 
 Pct Recovery = 119%  Analysis Date = 08/01/14 
 Pct Recovery = 119%  Analysis Date = 07/28/14 
 Pct Recovery = 119%  Analysis Date = 07/28/14 
 Pct Recovery = 119%  Analysis Date = 07/24/14 
 Pct Recovery = 119%  Analysis Date = 07/24/14 
 Pct Recovery = 119%  Analysis Date = 07/20/14 
 Pct Recovery = 120%  Analysis Date = 07/20/14 
 Pct Recovery = 120%  Analysis Date = 07/16/14 
 Pct Recovery = 120%  Analysis Date = 07/16/14 
 Pct Recovery = 120%  Analysis Date = 07/12/14 
 Pct Recovery = 120%  Analysis Date = 07/12/14 
 Pct Recovery = 120%  Analysis Date = 07/08/14 
 Pct Recovery = 121%  Analysis Date = 07/08/14 
 Pct Recovery = 121%  Analysis Date = 07/03/14 
 Pct Recovery = 121%  Analysis Date = 07/03/14 
 Pct Recovery = 121%  Analysis Date = 06/29/14 
 Pct Recovery = 121%  Analysis Date = 06/29/14 
 Pct Recovery = 121%  Analysis Date = 06/25/14 
 Pct Recovery = 122%  Analysis Date = 06/25/14 
 Pct Recovery = 122%  Analysis Date = 06/21/14 
 Pct Recovery = 122%  Analysis Date = 06/21/14 
 Pct Recovery = 122%  Analysis Date = 06/17/14 
 Pct Recovery = 122%  Analysis Date = 06/17/14 
 Pct Recovery = 122%  Analysis Date = 06/13/14 
 Pct Recovery = 122%  Analysis Date = 06/13/14 
 Pct Recovery = 122%  Analysis Date = 06/09/14 
 Pct Recovery = 123%  Analysis Date = 06/09/14 
 Pct Recovery = 123%  Analysis Date = 06/04/14 
 Pct Recovery = 123%  Analysis Date = 06/04/14 
 Pct Recovery = 123%  Analysis Date = 05/31/14 
 Pct Recovery = 123%  Analysis Date = 05/31/14 
 Pct Recovery = 123%  Analysis Date = 05/27/14 
 Pct Recovery = 124%  Analysis Date = 05/27/14 
 Pct Recovery = 124%  Analysis Date = 05/23/14 
 Pct Recovery = 124%  Analysis Date = 05/23/14 
 Pct Recovery = 124%  Analysis Date = 05/19/14 
 Pct Recovery = 124%  Analysis Date = 05/19/14 
 Pct Recovery = 124%  Analysis Date = 05/15/14 
 Pct Recovery = 125%  Analysis Date = 05/15/14 
 Pct Recovery = 125%  Analysis Date = 05/11/14 
 Pct Recovery = 125%  Analysis Date = 05/11/14 
 Pct Recovery = 125%  Analysis Date = 05/07/14 
 Pct Recovery = 125%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
ISOPHORONE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 38 92% 23% 85% 25%
Total 38 92% 23% 85% 25%

Sample Statistics
ISOPHORONE

Characteristic N % % Basis
Plotted 38 100% Spiked
Estimated Values 2 5% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 38 .  
False Negatives 0 0% 0 out of 38
Not Spiked 17 .  
False Positives 0 0% 0 out of 17

BQS OBSP Determination:
ISOPROPYL ALCOHOL
METHOD: 4437 , TESTIDCODE: 77015GM016
Open Data Set

 Analysis Date = 08/11/16 
 SpikeMix = Phenova B20160303: 25 µl & Supelco LC20145V: 25 µl & NSI 041416HVOC: 25 µl 
 Pct Recovery = 904%  Analysis Date = 07/06/16 
 SpikeMix = Phenova B20160303: 15 µl & Accu 216041354: 15 µl & NSI 041416HVOC: 15 µl 
 Pct Recovery = 792%  Analysis Date = 07/06/16 
 SpikeMix = Accu 216041354: 40 µl & NSI 041516: 40 µl & NSI 041416HVOC: 40 µl 
 Pct Recovery = 104%  Analysis Date = 07/29/16 
 SpikeMix = Supelco LC20145V: 40 µl & NSI 041516: 40 µl & NSI 041416HVOC: 40 µl 
 Pct Recovery = 103%  Analysis Date = 03/19/15 
 SpikeMix = Supelco LC06437: 20 µl & NSI 031814: 20 µl 
 Pct Recovery = 103%  Analysis Date = 01/10/15 
 SpikeMix = Abs 032014: 20 µl & ERA 0321-14-05A: 20 µl 
 Pct Recovery = 120%  Analysis Date = 08/20/14 
 SpikeMix = Supelco LC06437: 20 µl & Abs 032014: 20 µl 
 Pct Recovery = 113%  Analysis Date = 07/23/14 
 SpikeMix = Accu 214031128: 20 µl & Abs 032014: 20 µl 
 Pct Recovery = 111%  Analysis Date = 07/03/14 
 SpikeMix = Abs 032014: 20 µl & ChemService 2615700: 20 µl 
 Pct Recovery = 110%  Analysis Date = 06/06/14 
 SpikeMix = NSI 031814: 20 µl & ChemService 2615700: 20 µl 
 Pct Recovery = 116%  Analysis Date = 05/07/14 
 SpikeMix = NSI 031814: 20 µl & Accu 214031128: 20 µl 
 Pct Recovery = 107%  Analysis Date = 05/21/16 
 SpikeMix = Supelco LC20145V: 25 µl & NSI 041516: 25 µl & NSI 041416HVOC: 25 µl 
 Pct Recovery = 123%  Analysis Date = 01/22/16 
 SpikeMix = NSI 050515HVOC: 25 µl & ERA 0601-15-05: 25 µl 
 Pct Recovery = 96%  Analysis Date = 10/09/15 
 SpikeMix = Supelco LC13544: 25 µl & NSI 050515HVOC: 25 µl 
 Pct Recovery = 100%  Analysis Date = 06/25/15 
 SpikeMix = ChemService 3818700: 25 µl & NSI 050515HVOC: 25 µl 
 Pct Recovery = 85%  Analysis Date = 04/25/15 
 SpikeMix = Abs 032014: 10 µl & ERA 0321-14-05A: 10 µl 
 Pct Recovery = 88%  Analysis Date = 12/13/14 
 SpikeMix = Accu 214031128: 10 µl & NSI 031814: 10 µl 
 Pct Recovery = 106%  Analysis Date = 09/11/14 
 SpikeMix = Accu 214031128: 10 µl & Abs 032014: 10 µl 
 Pct Recovery = 122%  Analysis Date = 07/30/14 
 SpikeMix = NSI 031814: 10 µl & ChemService 2615700: 10 µl 
 Pct Recovery = 124%  Analysis Date = 06/17/14 
 SpikeMix = Supelco LC06437: 10 µl & Abs 032014: 10 µl 
 Pct Recovery = 128%  Analysis Date = 08/12/16 
 SpikeMix = Accu 216041354: 15 µl & Abs 060916HVOC: 15 µl 
 Pct Recovery = 94%  Analysis Date = 06/23/16 
 SpikeMix = . 
 Pct Recovery = 69%  Analysis Date = 05/20/16 
 SpikeMix = Accu 216041354: 15 µl & NSI 041516: 15 µl & Accu 216041225: 15 µl 
 Pct Recovery = 152%  Analysis Date = 07/27/16 
 SpikeMix = ChemService 5082800: 15 µl & Supelco LC20145V: 15 µl & Accu 216041225: 15 µl 
 Pct Recovery = 81%  Analysis Date = 09/05/15 
 SpikeMix = Accu 215041338: 15 µl & NSI 050515HVOC: 15 µl 
 Pct Recovery = 94%  Analysis Date = 07/30/15 
 SpikeMix = Supelco LC13544: 15 µl & NSI 050515HVOC: 15 µl 
 Pct Recovery = 85%  Analysis Date = 06/16/15 
 SpikeMix = ChemService 3818700: 15 µl & NSI 050515HVOC: 15 µl 
 Pct Recovery = 86%  Analysis Date = 11/25/15 
 SpikeMix = Accu 215041338: 15 µl & Abs 040315: 15 µl 
 Pct Recovery = 90%  Analysis Date = 09/24/15 
 SpikeMix = Abs 040315: 15 µl & ERA 0601-15-05: 15 µl 
 Pct Recovery = 93%  Analysis Date = 03/22/16 
 SpikeMix = Supelco LC13544: 10 µl & NSI 050515HVOC: 10 µl 
 Pct Recovery = 138%  Analysis Date = 12/05/15 
 SpikeMix = NSI 050515HVOC: 10 µl & ERA 0601-15-05: 10 µl 
 Pct Recovery = 105%  Analysis Date = 04/09/16 
 SpikeMix = Abs 040315: 10 µl & ChemService 3818700: 10 µl 
 Pct Recovery = 133%  Analysis Date = 01/05/16 
 SpikeMix = Accu 215041338: 10 µl & Abs 040315: 10 µl 
 Pct Recovery = 134%  Analysis Date = 10/23/15 
 SpikeMix = Abs 040315: 10 µl & ChemService 3818700: 10 µl 
 Pct Recovery = 97%  Analysis Date = 08/14/15 
 SpikeMix = Abs 040315: 10 µl & ERA 0601-15-05: 10 µl 
 Pct Recovery = 81%  Analysis Date = 05/05/15 
 SpikeMix = Supelco LC13544: 10 µl & Abs 040315: 10 µl 
 Pct Recovery = 108%  Analysis Date = 04/26/16 
 Pct Recovery = 202%  Analysis Date = 04/26/16 
 Pct Recovery = 202%  Analysis Date = 04/22/16 
 Pct Recovery = 198%  Analysis Date = 04/22/16 
 Pct Recovery = 198%  Analysis Date = 04/18/16 
 Pct Recovery = 194%  Analysis Date = 04/18/16 
 Pct Recovery = 194%  Analysis Date = 04/13/16 
 Pct Recovery = 190%  Analysis Date = 04/13/16 
 Pct Recovery = 190%  Analysis Date = 04/09/16 
 Pct Recovery = 186%  Analysis Date = 04/09/16 
 Pct Recovery = 186%  Analysis Date = 04/05/16 
 Pct Recovery = 184%  Analysis Date = 04/05/16 
 Pct Recovery = 184%  Analysis Date = 04/01/16 
 Pct Recovery = 181%  Analysis Date = 04/01/16 
 Pct Recovery = 181%  Analysis Date = 03/28/16 
 Pct Recovery = 178%  Analysis Date = 03/28/16 
 Pct Recovery = 178%  Analysis Date = 03/24/16 
 Pct Recovery = 176%  Analysis Date = 03/24/16 
 Pct Recovery = 176%  Analysis Date = 03/20/16 
 Pct Recovery = 173%  Analysis Date = 03/20/16 
 Pct Recovery = 173%  Analysis Date = 03/15/16 
 Pct Recovery = 171%  Analysis Date = 03/15/16 
 Pct Recovery = 171%  Analysis Date = 03/11/16 
 Pct Recovery = 168%  Analysis Date = 03/11/16 
 Pct Recovery = 168%  Analysis Date = 03/07/16 
 Pct Recovery = 165%  Analysis Date = 03/07/16 
 Pct Recovery = 165%  Analysis Date = 03/03/16 
 Pct Recovery = 163%  Analysis Date = 03/03/16 
 Pct Recovery = 163%  Analysis Date = 02/28/16 
 Pct Recovery = 160%  Analysis Date = 02/28/16 
 Pct Recovery = 160%  Analysis Date = 02/24/16 
 Pct Recovery = 158%  Analysis Date = 02/24/16 
 Pct Recovery = 158%  Analysis Date = 02/20/16 
 Pct Recovery = 155%  Analysis Date = 02/20/16 
 Pct Recovery = 155%  Analysis Date = 02/15/16 
 Pct Recovery = 153%  Analysis Date = 02/15/16 
 Pct Recovery = 153%  Analysis Date = 02/11/16 
 Pct Recovery = 150%  Analysis Date = 02/11/16 
 Pct Recovery = 150%  Analysis Date = 02/07/16 
 Pct Recovery = 147%  Analysis Date = 02/07/16 
 Pct Recovery = 147%  Analysis Date = 02/03/16 
 Pct Recovery = 145%  Analysis Date = 02/03/16 
 Pct Recovery = 145%  Analysis Date = 01/30/16 
 Pct Recovery = 142%  Analysis Date = 01/30/16 
 Pct Recovery = 142%  Analysis Date = 01/26/16 
 Pct Recovery = 140%  Analysis Date = 01/26/16 
 Pct Recovery = 140%  Analysis Date = 01/22/16 
 Pct Recovery = 137%  Analysis Date = 01/22/16 
 Pct Recovery = 137%  Analysis Date = 01/17/16 
 Pct Recovery = 134%  Analysis Date = 01/17/16 
 Pct Recovery = 134%  Analysis Date = 01/13/16 
 Pct Recovery = 132%  Analysis Date = 01/13/16 
 Pct Recovery = 132%  Analysis Date = 01/09/16 
 Pct Recovery = 129%  Analysis Date = 01/09/16 
 Pct Recovery = 129%  Analysis Date = 01/05/16 
 Pct Recovery = 127%  Analysis Date = 01/05/16 
 Pct Recovery = 127%  Analysis Date = 01/01/16 
 Pct Recovery = 124%  Analysis Date = 01/01/16 
 Pct Recovery = 124%  Analysis Date = 12/28/15 
 Pct Recovery = 122%  Analysis Date = 12/28/15 
 Pct Recovery = 122%  Analysis Date = 12/24/15 
 Pct Recovery = 119%  Analysis Date = 12/24/15 
 Pct Recovery = 119%  Analysis Date = 12/20/15 
 Pct Recovery = 116%  Analysis Date = 12/20/15 
 Pct Recovery = 116%  Analysis Date = 12/15/15 
 Pct Recovery = 114%  Analysis Date = 12/15/15 
 Pct Recovery = 114%  Analysis Date = 12/11/15 
 Pct Recovery = 111%  Analysis Date = 12/11/15 
 Pct Recovery = 111%  Analysis Date = 12/07/15 
 Pct Recovery = 109%  Analysis Date = 12/07/15 
 Pct Recovery = 109%  Analysis Date = 12/03/15 
 Pct Recovery = 107%  Analysis Date = 12/03/15 
 Pct Recovery = 107%  Analysis Date = 11/29/15 
 Pct Recovery = 106%  Analysis Date = 11/29/15 
 Pct Recovery = 106%  Analysis Date = 11/25/15 
 Pct Recovery = 106%  Analysis Date = 11/25/15 
 Pct Recovery = 106%  Analysis Date = 11/21/15 
 Pct Recovery = 105%  Analysis Date = 11/21/15 
 Pct Recovery = 105%  Analysis Date = 11/16/15 
 Pct Recovery = 104%  Analysis Date = 11/16/15 
 Pct Recovery = 104%  Analysis Date = 11/12/15 
 Pct Recovery = 104%  Analysis Date = 11/12/15 
 Pct Recovery = 104%  Analysis Date = 11/08/15 
 Pct Recovery = 103%  Analysis Date = 11/08/15 
 Pct Recovery = 103%  Analysis Date = 11/04/15 
 Pct Recovery = 103%  Analysis Date = 11/04/15 
 Pct Recovery = 103%  Analysis Date = 10/31/15 
 Pct Recovery = 102%  Analysis Date = 10/31/15 
 Pct Recovery = 102%  Analysis Date = 10/27/15 
 Pct Recovery = 102%  Analysis Date = 10/27/15 
 Pct Recovery = 102%  Analysis Date = 10/23/15 
 Pct Recovery = 101%  Analysis Date = 10/23/15 
 Pct Recovery = 101%  Analysis Date = 10/18/15 
 Pct Recovery = 101%  Analysis Date = 10/18/15 
 Pct Recovery = 101%  Analysis Date = 10/14/15 
 Pct Recovery = 100%  Analysis Date = 10/14/15 
 Pct Recovery = 100%  Analysis Date = 10/10/15 
 Pct Recovery = 100%  Analysis Date = 10/10/15 
 Pct Recovery = 100%  Analysis Date = 10/06/15 
 Pct Recovery = 99%  Analysis Date = 10/06/15 
 Pct Recovery = 99%  Analysis Date = 10/02/15 
 Pct Recovery = 99%  Analysis Date = 10/02/15 
 Pct Recovery = 99%  Analysis Date = 09/28/15 
 Pct Recovery = 98%  Analysis Date = 09/28/15 
 Pct Recovery = 98%  Analysis Date = 09/24/15 
 Pct Recovery = 98%  Analysis Date = 09/24/15 
 Pct Recovery = 98%  Analysis Date = 09/19/15 
 Pct Recovery = 98%  Analysis Date = 09/19/15 
 Pct Recovery = 98%  Analysis Date = 09/15/15 
 Pct Recovery = 97%  Analysis Date = 09/15/15 
 Pct Recovery = 97%  Analysis Date = 09/11/15 
 Pct Recovery = 97%  Analysis Date = 09/11/15 
 Pct Recovery = 97%  Analysis Date = 09/07/15 
 Pct Recovery = 96%  Analysis Date = 09/07/15 
 Pct Recovery = 96%  Analysis Date = 09/03/15 
 Pct Recovery = 96%  Analysis Date = 09/03/15 
 Pct Recovery = 96%  Analysis Date = 08/30/15 
 Pct Recovery = 96%  Analysis Date = 08/30/15 
 Pct Recovery = 96%  Analysis Date = 08/26/15 
 Pct Recovery = 96%  Analysis Date = 08/26/15 
 Pct Recovery = 96%  Analysis Date = 08/21/15 
 Pct Recovery = 96%  Analysis Date = 08/21/15 
 Pct Recovery = 96%  Analysis Date = 08/17/15 
 Pct Recovery = 96%  Analysis Date = 08/17/15 
 Pct Recovery = 96%  Analysis Date = 08/13/15 
 Pct Recovery = 96%  Analysis Date = 08/13/15 
 Pct Recovery = 96%  Analysis Date = 08/09/15 
 Pct Recovery = 96%  Analysis Date = 08/09/15 
 Pct Recovery = 96%  Analysis Date = 08/05/15 
 Pct Recovery = 96%  Analysis Date = 08/05/15 
 Pct Recovery = 96%  Analysis Date = 08/01/15 
 Pct Recovery = 96%  Analysis Date = 08/01/15 
 Pct Recovery = 96%  Analysis Date = 07/28/15 
 Pct Recovery = 96%  Analysis Date = 07/28/15 
 Pct Recovery = 96%  Analysis Date = 07/23/15 
 Pct Recovery = 96%  Analysis Date = 07/23/15 
 Pct Recovery = 96%  Analysis Date = 07/19/15 
 Pct Recovery = 96%  Analysis Date = 07/19/15 
 Pct Recovery = 96%  Analysis Date = 07/15/15 
 Pct Recovery = 96%  Analysis Date = 07/15/15 
 Pct Recovery = 96%  Analysis Date = 07/11/15 
 Pct Recovery = 96%  Analysis Date = 07/11/15 
 Pct Recovery = 96%  Analysis Date = 07/07/15 
 Pct Recovery = 96%  Analysis Date = 07/07/15 
 Pct Recovery = 96%  Analysis Date = 07/03/15 
 Pct Recovery = 96%  Analysis Date = 07/03/15 
 Pct Recovery = 96%  Analysis Date = 06/29/15 
 Pct Recovery = 96%  Analysis Date = 06/29/15 
 Pct Recovery = 96%  Analysis Date = 06/24/15 
 Pct Recovery = 96%  Analysis Date = 06/24/15 
 Pct Recovery = 96%  Analysis Date = 06/20/15 
 Pct Recovery = 96%  Analysis Date = 06/20/15 
 Pct Recovery = 96%  Analysis Date = 06/16/15 
 Pct Recovery = 96%  Analysis Date = 06/16/15 
 Pct Recovery = 96%  Analysis Date = 06/12/15 
 Pct Recovery = 97%  Analysis Date = 06/12/15 
 Pct Recovery = 97%  Analysis Date = 06/08/15 
 Pct Recovery = 97%  Analysis Date = 06/08/15 
 Pct Recovery = 97%  Analysis Date = 06/04/15 
 Pct Recovery = 97%  Analysis Date = 06/04/15 
 Pct Recovery = 97%  Analysis Date = 05/31/15 
 Pct Recovery = 97%  Analysis Date = 05/31/15 
 Pct Recovery = 97%  Analysis Date = 05/27/15 
 Pct Recovery = 97%  Analysis Date = 05/27/15 
 Pct Recovery = 97%  Analysis Date = 05/22/15 
 Pct Recovery = 98%  Analysis Date = 05/22/15 
 Pct Recovery = 98%  Analysis Date = 05/18/15 
 Pct Recovery = 98%  Analysis Date = 05/18/15 
 Pct Recovery = 98%  Analysis Date = 05/14/15 
 Pct Recovery = 98%  Analysis Date = 05/14/15 
 Pct Recovery = 98%  Analysis Date = 05/10/15 
 Pct Recovery = 98%  Analysis Date = 05/10/15 
 Pct Recovery = 98%  Analysis Date = 05/06/15 
 Pct Recovery = 98%  Analysis Date = 05/06/15 
 Pct Recovery = 98%  Analysis Date = 05/02/15 
 Pct Recovery = 99%  Analysis Date = 05/02/15 
 Pct Recovery = 99%  Analysis Date = 04/28/15 
 Pct Recovery = 99%  Analysis Date = 04/28/15 
 Pct Recovery = 99%  Analysis Date = 04/23/15 
 Pct Recovery = 99%  Analysis Date = 04/23/15 
 Pct Recovery = 99%  Analysis Date = 04/19/15 
 Pct Recovery = 99%  Analysis Date = 04/19/15 
 Pct Recovery = 99%  Analysis Date = 04/15/15 
 Pct Recovery = 100%  Analysis Date = 04/15/15 
 Pct Recovery = 100%  Analysis Date = 04/11/15 
 Pct Recovery = 100%  Analysis Date = 04/11/15 
 Pct Recovery = 100%  Analysis Date = 04/07/15 
 Pct Recovery = 100%  Analysis Date = 04/07/15 
 Pct Recovery = 100%  Analysis Date = 04/03/15 
 Pct Recovery = 100%  Analysis Date = 04/03/15 
 Pct Recovery = 100%  Analysis Date = 03/30/15 
 Pct Recovery = 101%  Analysis Date = 03/30/15 
 Pct Recovery = 101%  Analysis Date = 03/25/15 
 Pct Recovery = 101%  Analysis Date = 03/25/15 
 Pct Recovery = 101%  Analysis Date = 03/21/15 
 Pct Recovery = 101%  Analysis Date = 03/21/15 
 Pct Recovery = 101%  Analysis Date = 03/17/15 
 Pct Recovery = 101%  Analysis Date = 03/17/15 
 Pct Recovery = 101%  Analysis Date = 03/13/15 
 Pct Recovery = 102%  Analysis Date = 03/13/15 
 Pct Recovery = 102%  Analysis Date = 03/09/15 
 Pct Recovery = 102%  Analysis Date = 03/09/15 
 Pct Recovery = 102%  Analysis Date = 03/05/15 
 Pct Recovery = 102%  Analysis Date = 03/05/15 
 Pct Recovery = 102%  Analysis Date = 03/01/15 
 Pct Recovery = 103%  Analysis Date = 03/01/15 
 Pct Recovery = 103%  Analysis Date = 02/24/15 
 Pct Recovery = 103%  Analysis Date = 02/24/15 
 Pct Recovery = 103%  Analysis Date = 02/20/15 
 Pct Recovery = 103%  Analysis Date = 02/20/15 
 Pct Recovery = 103%  Analysis Date = 02/16/15 
 Pct Recovery = 103%  Analysis Date = 02/16/15 
 Pct Recovery = 103%  Analysis Date = 02/12/15 
 Pct Recovery = 104%  Analysis Date = 02/12/15 
 Pct Recovery = 104%  Analysis Date = 02/08/15 
 Pct Recovery = 104%  Analysis Date = 02/08/15 
 Pct Recovery = 104%  Analysis Date = 02/04/15 
 Pct Recovery = 104%  Analysis Date = 02/04/15 
 Pct Recovery = 104%  Analysis Date = 01/31/15 
 Pct Recovery = 104%  Analysis Date = 01/31/15 
 Pct Recovery = 104%  Analysis Date = 01/26/15 
 Pct Recovery = 105%  Analysis Date = 01/26/15 
 Pct Recovery = 105%  Analysis Date = 01/22/15 
 Pct Recovery = 105%  Analysis Date = 01/22/15 
 Pct Recovery = 105%  Analysis Date = 01/18/15 
 Pct Recovery = 105%  Analysis Date = 01/18/15 
 Pct Recovery = 105%  Analysis Date = 01/14/15 
 Pct Recovery = 106%  Analysis Date = 01/14/15 
 Pct Recovery = 106%  Analysis Date = 01/10/15 
 Pct Recovery = 106%  Analysis Date = 01/10/15 
 Pct Recovery = 106%  Analysis Date = 01/06/15 
 Pct Recovery = 106%  Analysis Date = 01/06/15 
 Pct Recovery = 106%  Analysis Date = 01/02/15 
 Pct Recovery = 106%  Analysis Date = 01/02/15 
 Pct Recovery = 106%  Analysis Date = 12/28/14 
 Pct Recovery = 107%  Analysis Date = 12/28/14 
 Pct Recovery = 107%  Analysis Date = 12/24/14 
 Pct Recovery = 107%  Analysis Date = 12/24/14 
 Pct Recovery = 107%  Analysis Date = 12/20/14 
 Pct Recovery = 107%  Analysis Date = 12/20/14 
 Pct Recovery = 107%  Analysis Date = 12/16/14 
 Pct Recovery = 108%  Analysis Date = 12/16/14 
 Pct Recovery = 108%  Analysis Date = 12/12/14 
 Pct Recovery = 108%  Analysis Date = 12/12/14 
 Pct Recovery = 108%  Analysis Date = 12/08/14 
 Pct Recovery = 108%  Analysis Date = 12/08/14 
 Pct Recovery = 108%  Analysis Date = 12/04/14 
 Pct Recovery = 108%  Analysis Date = 12/04/14 
 Pct Recovery = 108%  Analysis Date = 11/29/14 
 Pct Recovery = 108%  Analysis Date = 11/29/14 
 Pct Recovery = 108%  Analysis Date = 11/25/14 
 Pct Recovery = 109%  Analysis Date = 11/25/14 
 Pct Recovery = 109%  Analysis Date = 11/21/14 
 Pct Recovery = 109%  Analysis Date = 11/21/14 
 Pct Recovery = 109%  Analysis Date = 11/17/14 
 Pct Recovery = 109%  Analysis Date = 11/17/14 
 Pct Recovery = 109%  Analysis Date = 11/13/14 
 Pct Recovery = 109%  Analysis Date = 11/13/14 
 Pct Recovery = 109%  Analysis Date = 11/09/14 
 Pct Recovery = 110%  Analysis Date = 11/09/14 
 Pct Recovery = 110%  Analysis Date = 11/05/14 
 Pct Recovery = 110%  Analysis Date = 11/05/14 
 Pct Recovery = 110%  Analysis Date = 11/01/14 
 Pct Recovery = 110%  Analysis Date = 11/01/14 
 Pct Recovery = 110%  Analysis Date = 10/27/14 
 Pct Recovery = 110%  Analysis Date = 10/27/14 
 Pct Recovery = 110%  Analysis Date = 10/23/14 
 Pct Recovery = 111%  Analysis Date = 10/23/14 
 Pct Recovery = 111%  Analysis Date = 10/19/14 
 Pct Recovery = 111%  Analysis Date = 10/19/14 
 Pct Recovery = 111%  Analysis Date = 10/15/14 
 Pct Recovery = 111%  Analysis Date = 10/15/14 
 Pct Recovery = 111%  Analysis Date = 10/11/14 
 Pct Recovery = 111%  Analysis Date = 10/11/14 
 Pct Recovery = 111%  Analysis Date = 10/07/14 
 Pct Recovery = 112%  Analysis Date = 10/07/14 
 Pct Recovery = 112%  Analysis Date = 10/03/14 
 Pct Recovery = 112%  Analysis Date = 10/03/14 
 Pct Recovery = 112%  Analysis Date = 09/28/14 
 Pct Recovery = 112%  Analysis Date = 09/28/14 
 Pct Recovery = 112%  Analysis Date = 09/24/14 
 Pct Recovery = 112%  Analysis Date = 09/24/14 
 Pct Recovery = 112%  Analysis Date = 09/20/14 
 Pct Recovery = 112%  Analysis Date = 09/20/14 
 Pct Recovery = 112%  Analysis Date = 09/16/14 
 Pct Recovery = 113%  Analysis Date = 09/16/14 
 Pct Recovery = 113%  Analysis Date = 09/12/14 
 Pct Recovery = 113%  Analysis Date = 09/12/14 
 Pct Recovery = 113%  Analysis Date = 09/08/14 
 Pct Recovery = 113%  Analysis Date = 09/08/14 
 Pct Recovery = 113%  Analysis Date = 09/04/14 
 Pct Recovery = 113%  Analysis Date = 09/04/14 
 Pct Recovery = 113%  Analysis Date = 08/30/14 
 Pct Recovery = 114%  Analysis Date = 08/30/14 
 Pct Recovery = 114%  Analysis Date = 08/26/14 
 Pct Recovery = 114%  Analysis Date = 08/26/14 
 Pct Recovery = 114%  Analysis Date = 08/22/14 
 Pct Recovery = 114%  Analysis Date = 08/22/14 
 Pct Recovery = 114%  Analysis Date = 08/18/14 
 Pct Recovery = 114%  Analysis Date = 08/18/14 
 Pct Recovery = 114%  Analysis Date = 08/14/14 
 Pct Recovery = 115%  Analysis Date = 08/14/14 
 Pct Recovery = 115%  Analysis Date = 08/10/14 
 Pct Recovery = 115%  Analysis Date = 08/10/14 
 Pct Recovery = 115%  Analysis Date = 08/06/14 
 Pct Recovery = 115%  Analysis Date = 08/06/14 
 Pct Recovery = 115%  Analysis Date = 08/01/14 
 Pct Recovery = 115%  Analysis Date = 08/01/14 
 Pct Recovery = 115%  Analysis Date = 07/28/14 
 Pct Recovery = 115%  Analysis Date = 07/28/14 
 Pct Recovery = 115%  Analysis Date = 07/24/14 
 Pct Recovery = 116%  Analysis Date = 07/24/14 
 Pct Recovery = 116%  Analysis Date = 07/20/14 
 Pct Recovery = 116%  Analysis Date = 07/20/14 
 Pct Recovery = 116%  Analysis Date = 07/16/14 
 Pct Recovery = 116%  Analysis Date = 07/16/14 
 Pct Recovery = 116%  Analysis Date = 07/12/14 
 Pct Recovery = 116%  Analysis Date = 07/12/14 
 Pct Recovery = 116%  Analysis Date = 07/08/14 
 Pct Recovery = 117%  Analysis Date = 07/08/14 
 Pct Recovery = 117%  Analysis Date = 07/03/14 
 Pct Recovery = 117%  Analysis Date = 07/03/14 
 Pct Recovery = 117%  Analysis Date = 06/29/14 
 Pct Recovery = 117%  Analysis Date = 06/29/14 
 Pct Recovery = 117%  Analysis Date = 06/25/14 
 Pct Recovery = 117%  Analysis Date = 06/25/14 
 Pct Recovery = 117%  Analysis Date = 06/21/14 
 Pct Recovery = 117%  Analysis Date = 06/21/14 
 Pct Recovery = 117%  Analysis Date = 06/17/14 
 Pct Recovery = 118%  Analysis Date = 06/17/14 
 Pct Recovery = 118%  Analysis Date = 06/13/14 
 Pct Recovery = 118%  Analysis Date = 06/13/14 
 Pct Recovery = 118%  Analysis Date = 06/09/14 
 Pct Recovery = 118%  Analysis Date = 06/09/14 
 Pct Recovery = 118%  Analysis Date = 06/04/14 
 Pct Recovery = 118%  Analysis Date = 06/04/14 
 Pct Recovery = 118%  Analysis Date = 05/31/14 
 Pct Recovery = 118%  Analysis Date = 05/31/14 
 Pct Recovery = 118%  Analysis Date = 05/27/14 
 Pct Recovery = 119%  Analysis Date = 05/27/14 
 Pct Recovery = 119%  Analysis Date = 05/23/14 
 Pct Recovery = 119%  Analysis Date = 05/23/14 
 Pct Recovery = 119%  Analysis Date = 05/19/14 
 Pct Recovery = 119%  Analysis Date = 05/19/14 
 Pct Recovery = 119%  Analysis Date = 05/15/14 
 Pct Recovery = 119%  Analysis Date = 05/15/14 
 Pct Recovery = 119%  Analysis Date = 05/11/14 
 Pct Recovery = 119%  Analysis Date = 05/11/14 
 Pct Recovery = 119%  Analysis Date = 05/07/14 
 Pct Recovery = 120%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
ISOPROPYL ALCOHOL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 36 147% 174% 106% 22%
Total 36 147% 174% 106% 22%

Sample Statistics
ISOPROPYL ALCOHOL

Characteristic N % % Basis
Plotted 36 100% Spiked
Estimated Values 1 3% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 36 .  
False Negatives 0 0% 0 out of 36
Not Spiked 19 .  
False Positives 4 21% 4 out of 19

BQS OBSP Determination:
METHYL ACETATE
METHOD: 4437 , TESTIDCODE: 77032GM016
Open Data Set

 Analysis Date = 07/29/16 
 SpikeMix = Supelco LC20145V: 40 µl & NSI 041516: 40 µl & NSI 041416HVOC: 40 µl 
 Pct Recovery = 88%  Analysis Date = 07/06/16 
 SpikeMix = Accu 216041354: 40 µl & NSI 041516: 40 µl & NSI 041416HVOC: 40 µl 
 Pct Recovery = 74%  Analysis Date = 08/11/16 
 SpikeMix = Phenova B20160303: 25 µl & Supelco LC20145V: 25 µl & NSI 041416HVOC: 25 µl 
 Pct Recovery = 75%  Analysis Date = 07/14/16 
 SpikeMix = NSI 041516: 25 µl & ChemService 5082800: 25 µl & NSI 041416HVOC: 25 µl 
 Pct Recovery = 102%  Analysis Date = 05/21/16 
 SpikeMix = Supelco LC20145V: 25 µl & NSI 041516: 25 µl & NSI 041416HVOC: 25 µl 
 Pct Recovery = 94%  Analysis Date = 03/19/15 
 SpikeMix = Supelco LC06437: 20 µl & NSI 031814: 20 µl 
 Pct Recovery = 41%  Analysis Date = 01/10/15 
 SpikeMix = Abs 032014: 20 µl & ERA 0321-14-05A: 20 µl 
 Pct Recovery = 38%  Analysis Date = 08/20/14 
 SpikeMix = Supelco LC06437: 20 µl & Abs 032014: 20 µl 
 Pct Recovery = 41%  Analysis Date = 07/23/14 
 SpikeMix = Accu 214031128: 20 µl & Abs 032014: 20 µl 
 Pct Recovery = 39%  Analysis Date = 07/03/14 
 SpikeMix = Abs 032014: 20 µl & ChemService 2615700: 20 µl 
 Pct Recovery = 50%  Analysis Date = 06/06/14 
 SpikeMix = NSI 031814: 20 µl & ChemService 2615700: 20 µl 
 Pct Recovery = 62%  Analysis Date = 05/07/14 
 SpikeMix = NSI 031814: 20 µl & Accu 214031128: 20 µl 
 Pct Recovery = 47%  Analysis Date = 01/22/16 
 SpikeMix = NSI 050515HVOC: 25 µl & ERA 0601-15-05: 25 µl 
 Pct Recovery = 127%  Analysis Date = 10/09/15 
 SpikeMix = ERA 0601-15-05: 25 µl & Accu 215041338: 25 µl 
 Pct Recovery = 109%  Analysis Date = 06/26/15 
 SpikeMix = ChemService 3818700: 25 µl & Accu 215041338: 25 µl 
 Pct Recovery = 113%  Analysis Date = 06/25/15 
 SpikeMix = ChemService 3818700: 25 µl & NSI 050515HVOC: 25 µl 
 Pct Recovery = 94%  Analysis Date = 07/06/16 
 SpikeMix = Phenova B20160303: 15 µl & Accu 216041354: 15 µl & NSI 041416HVOC: 15 µl 
 Pct Recovery = 77%  Analysis Date = 06/03/16 
 SpikeMix = NSI 041516: 15 µl & Phenova B20160303: 15 µl & NSI 041416HVOC: 15 µl 
 Pct Recovery = 82%  Analysis Date = 07/27/16 
 SpikeMix = ChemService 5082800: 15 µl & Supelco LC20145V: 15 µl & Accu 216041225: 15 µl 
 Pct Recovery = 98%  Analysis Date = 05/20/16 
 SpikeMix = Accu 216041354: 15 µl & NSI 041516: 15 µl & Accu 216041225: 15 µl 
 Pct Recovery = 112%  Analysis Date = 04/28/16 
 SpikeMix = ChemService 3818700: 15 µl & Supelco LC13544: 15 µl 
 Pct Recovery = 142%  Analysis Date = 09/24/15 
 SpikeMix = Abs 040315: 15 µl & ERA 0601-15-05: 15 µl 
 Pct Recovery = 119%  Analysis Date = 08/24/15 
 SpikeMix = ERA 0601-15-05: 15 µl & Supelco LC13544: 15 µl 
 Pct Recovery = 130%  Analysis Date = 06/16/15 
 SpikeMix = ChemService 3818700: 15 µl & NSI 050515HVOC: 15 µl 
 Pct Recovery = 99%  Analysis Date = 05/14/15 
 SpikeMix = ChemService 3818700: 15 µl & Supelco LC13544: 15 µl 
 Pct Recovery = 103%  Analysis Date = 04/25/15 
 SpikeMix = Abs 032014: 10 µl & ERA 0321-14-05A: 10 µl 
 Pct Recovery = 105%  Analysis Date = 12/13/14 
 SpikeMix = Accu 214031128: 10 µl & NSI 031814: 10 µl 
 Pct Recovery = 37%  Analysis Date = 09/11/14 
 SpikeMix = Accu 214031128: 10 µl & Abs 032014: 10 µl 
 Pct Recovery = 45%  Analysis Date = 07/30/14 
 SpikeMix = NSI 031814: 10 µl & ChemService 2615700: 10 µl 
 Pct Recovery = 45%  Analysis Date = 06/17/14 
 SpikeMix = Supelco LC06437: 10 µl & Abs 032014: 10 µl 
 Pct Recovery = 40%  Analysis Date = 04/09/16 
 SpikeMix = Abs 040315: 10 µl & ChemService 3818700: 10 µl 
 Pct Recovery = 102%  Analysis Date = 02/12/16 
 SpikeMix = ERA 0601-15-05: 10 µl & Accu 215041338: 10 µl 
 Pct Recovery = 115%  Analysis Date = 12/10/15 
 SpikeMix = ChemService 3818700: 10 µl & Supelco LC13544: 10 µl 
 Pct Recovery = 139%  Analysis Date = 12/05/15 
 SpikeMix = NSI 050515HVOC: 10 µl & ERA 0601-15-05: 10 µl 
 Pct Recovery = 113%  Analysis Date = 11/14/15 
 SpikeMix = ERA 0601-15-05: 10 µl 
 Pct Recovery = 120%  Analysis Date = 10/23/15 
 SpikeMix = Abs 040315: 10 µl & ChemService 3818700: 10 µl 
 Pct Recovery = 101%  Analysis Date = 08/14/15 
 SpikeMix = Abs 040315: 10 µl & ERA 0601-15-05: 10 µl 
 Pct Recovery = 107%  Analysis Date = 05/20/15 
 SpikeMix = ChemService 3818700: 10 µl & Accu 215041338: 10 µl 
 Pct Recovery = 108%  Analysis Date = 08/10/16 
 Pct Recovery = 87%  Analysis Date = 08/06/16 
 Pct Recovery = 87%  Analysis Date = 08/06/16 
 Pct Recovery = 87%  Analysis Date = 08/02/16 
 Pct Recovery = 88%  Analysis Date = 08/02/16 
 Pct Recovery = 88%  Analysis Date = 07/29/16 
 Pct Recovery = 89%  Analysis Date = 07/29/16 
 Pct Recovery = 89%  Analysis Date = 07/25/16 
 Pct Recovery = 89%  Analysis Date = 07/25/16 
 Pct Recovery = 89%  Analysis Date = 07/21/16 
 Pct Recovery = 90%  Analysis Date = 07/21/16 
 Pct Recovery = 90%  Analysis Date = 07/17/16 
 Pct Recovery = 90%  Analysis Date = 07/17/16 
 Pct Recovery = 90%  Analysis Date = 07/13/16 
 Pct Recovery = 91%  Analysis Date = 07/13/16 
 Pct Recovery = 91%  Analysis Date = 07/08/16 
 Pct Recovery = 92%  Analysis Date = 07/08/16 
 Pct Recovery = 92%  Analysis Date = 07/04/16 
 Pct Recovery = 92%  Analysis Date = 07/04/16 
 Pct Recovery = 92%  Analysis Date = 06/30/16 
 Pct Recovery = 93%  Analysis Date = 06/30/16 
 Pct Recovery = 93%  Analysis Date = 06/26/16 
 Pct Recovery = 93%  Analysis Date = 06/26/16 
 Pct Recovery = 93%  Analysis Date = 06/22/16 
 Pct Recovery = 94%  Analysis Date = 06/22/16 
 Pct Recovery = 94%  Analysis Date = 06/18/16 
 Pct Recovery = 95%  Analysis Date = 06/18/16 
 Pct Recovery = 95%  Analysis Date = 06/14/16 
 Pct Recovery = 95%  Analysis Date = 06/14/16 
 Pct Recovery = 95%  Analysis Date = 06/09/16 
 Pct Recovery = 96%  Analysis Date = 06/09/16 
 Pct Recovery = 96%  Analysis Date = 06/05/16 
 Pct Recovery = 96%  Analysis Date = 06/05/16 
 Pct Recovery = 96%  Analysis Date = 06/01/16 
 Pct Recovery = 97%  Analysis Date = 06/01/16 
 Pct Recovery = 97%  Analysis Date = 05/28/16 
 Pct Recovery = 98%  Analysis Date = 05/28/16 
 Pct Recovery = 98%  Analysis Date = 05/24/16 
 Pct Recovery = 98%  Analysis Date = 05/24/16 
 Pct Recovery = 98%  Analysis Date = 05/20/16 
 Pct Recovery = 99%  Analysis Date = 05/20/16 
 Pct Recovery = 99%  Analysis Date = 05/16/16 
 Pct Recovery = 99%  Analysis Date = 05/16/16 
 Pct Recovery = 99%  Analysis Date = 05/12/16 
 Pct Recovery = 100%  Analysis Date = 05/12/16 
 Pct Recovery = 100%  Analysis Date = 05/07/16 
 Pct Recovery = 100%  Analysis Date = 05/07/16 
 Pct Recovery = 100%  Analysis Date = 05/03/16 
 Pct Recovery = 101%  Analysis Date = 05/03/16 
 Pct Recovery = 101%  Analysis Date = 04/29/16 
 Pct Recovery = 101%  Analysis Date = 04/29/16 
 Pct Recovery = 101%  Analysis Date = 04/25/16 
 Pct Recovery = 102%  Analysis Date = 04/25/16 
 Pct Recovery = 102%  Analysis Date = 04/21/16 
 Pct Recovery = 103%  Analysis Date = 04/21/16 
 Pct Recovery = 103%  Analysis Date = 04/17/16 
 Pct Recovery = 103%  Analysis Date = 04/17/16 
 Pct Recovery = 103%  Analysis Date = 04/13/16 
 Pct Recovery = 104%  Analysis Date = 04/13/16 
 Pct Recovery = 104%  Analysis Date = 04/08/16 
 Pct Recovery = 104%  Analysis Date = 04/08/16 
 Pct Recovery = 104%  Analysis Date = 04/04/16 
 Pct Recovery = 105%  Analysis Date = 04/04/16 
 Pct Recovery = 105%  Analysis Date = 03/31/16 
 Pct Recovery = 105%  Analysis Date = 03/31/16 
 Pct Recovery = 105%  Analysis Date = 03/27/16 
 Pct Recovery = 106%  Analysis Date = 03/27/16 
 Pct Recovery = 106%  Analysis Date = 03/23/16 
 Pct Recovery = 106%  Analysis Date = 03/23/16 
 Pct Recovery = 106%  Analysis Date = 03/19/16 
 Pct Recovery = 107%  Analysis Date = 03/19/16 
 Pct Recovery = 107%  Analysis Date = 03/15/16 
 Pct Recovery = 107%  Analysis Date = 03/15/16 
 Pct Recovery = 107%  Analysis Date = 03/11/16 
 Pct Recovery = 108%  Analysis Date = 03/11/16 
 Pct Recovery = 108%  Analysis Date = 03/06/16 
 Pct Recovery = 108%  Analysis Date = 03/06/16 
 Pct Recovery = 108%  Analysis Date = 03/02/16 
 Pct Recovery = 109%  Analysis Date = 03/02/16 
 Pct Recovery = 109%  Analysis Date = 02/27/16 
 Pct Recovery = 110%  Analysis Date = 02/27/16 
 Pct Recovery = 110%  Analysis Date = 02/23/16 
 Pct Recovery = 110%  Analysis Date = 02/23/16 
 Pct Recovery = 110%  Analysis Date = 02/19/16 
 Pct Recovery = 111%  Analysis Date = 02/19/16 
 Pct Recovery = 111%  Analysis Date = 02/15/16 
 Pct Recovery = 111%  Analysis Date = 02/15/16 
 Pct Recovery = 111%  Analysis Date = 02/11/16 
 Pct Recovery = 112%  Analysis Date = 02/11/16 
 Pct Recovery = 112%  Analysis Date = 02/06/16 
 Pct Recovery = 112%  Analysis Date = 02/06/16 
 Pct Recovery = 112%  Analysis Date = 02/02/16 
 Pct Recovery = 112%  Analysis Date = 02/02/16 
 Pct Recovery = 112%  Analysis Date = 01/29/16 
 Pct Recovery = 113%  Analysis Date = 01/29/16 
 Pct Recovery = 113%  Analysis Date = 01/25/16 
 Pct Recovery = 113%  Analysis Date = 01/25/16 
 Pct Recovery = 113%  Analysis Date = 01/21/16 
 Pct Recovery = 113%  Analysis Date = 01/21/16 
 Pct Recovery = 113%  Analysis Date = 01/17/16 
 Pct Recovery = 114%  Analysis Date = 01/17/16 
 Pct Recovery = 114%  Analysis Date = 01/13/16 
 Pct Recovery = 114%  Analysis Date = 01/13/16 
 Pct Recovery = 114%  Analysis Date = 01/08/16 
 Pct Recovery = 114%  Analysis Date = 01/08/16 
 Pct Recovery = 114%  Analysis Date = 01/04/16 
 Pct Recovery = 115%  Analysis Date = 01/04/16 
 Pct Recovery = 115%  Analysis Date = 12/31/15 
 Pct Recovery = 115%  Analysis Date = 12/31/15 
 Pct Recovery = 115%  Analysis Date = 12/27/15 
 Pct Recovery = 115%  Analysis Date = 12/27/15 
 Pct Recovery = 115%  Analysis Date = 12/23/15 
 Pct Recovery = 116%  Analysis Date = 12/23/15 
 Pct Recovery = 116%  Analysis Date = 12/19/15 
 Pct Recovery = 116%  Analysis Date = 12/19/15 
 Pct Recovery = 116%  Analysis Date = 12/15/15 
 Pct Recovery = 116%  Analysis Date = 12/15/15 
 Pct Recovery = 116%  Analysis Date = 12/11/15 
 Pct Recovery = 117%  Analysis Date = 12/11/15 
 Pct Recovery = 117%  Analysis Date = 12/06/15 
 Pct Recovery = 117%  Analysis Date = 12/06/15 
 Pct Recovery = 117%  Analysis Date = 12/02/15 
 Pct Recovery = 117%  Analysis Date = 12/02/15 
 Pct Recovery = 117%  Analysis Date = 11/28/15 
 Pct Recovery = 117%  Analysis Date = 11/28/15 
 Pct Recovery = 117%  Analysis Date = 11/24/15 
 Pct Recovery = 117%  Analysis Date = 11/24/15 
 Pct Recovery = 117%  Analysis Date = 11/20/15 
 Pct Recovery = 117%  Analysis Date = 11/20/15 
 Pct Recovery = 117%  Analysis Date = 11/16/15 
 Pct Recovery = 116%  Analysis Date = 11/16/15 
 Pct Recovery = 116%  Analysis Date = 11/12/15 
 Pct Recovery = 116%  Analysis Date = 11/12/15 
 Pct Recovery = 116%  Analysis Date = 11/07/15 
 Pct Recovery = 116%  Analysis Date = 11/07/15 
 Pct Recovery = 116%  Analysis Date = 11/03/15 
 Pct Recovery = 116%  Analysis Date = 11/03/15 
 Pct Recovery = 116%  Analysis Date = 10/30/15 
 Pct Recovery = 116%  Analysis Date = 10/30/15 
 Pct Recovery = 116%  Analysis Date = 10/26/15 
 Pct Recovery = 116%  Analysis Date = 10/26/15 
 Pct Recovery = 116%  Analysis Date = 10/22/15 
 Pct Recovery = 116%  Analysis Date = 10/22/15 
 Pct Recovery = 116%  Analysis Date = 10/18/15 
 Pct Recovery = 115%  Analysis Date = 10/18/15 
 Pct Recovery = 115%  Analysis Date = 10/14/15 
 Pct Recovery = 115%  Analysis Date = 10/14/15 
 Pct Recovery = 115%  Analysis Date = 10/10/15 
 Pct Recovery = 114%  Analysis Date = 10/10/15 
 Pct Recovery = 114%  Analysis Date = 10/05/15 
 Pct Recovery = 114%  Analysis Date = 10/05/15 
 Pct Recovery = 114%  Analysis Date = 10/01/15 
 Pct Recovery = 113%  Analysis Date = 10/01/15 
 Pct Recovery = 113%  Analysis Date = 09/27/15 
 Pct Recovery = 113%  Analysis Date = 09/27/15 
 Pct Recovery = 113%  Analysis Date = 09/23/15 
 Pct Recovery = 112%  Analysis Date = 09/23/15 
 Pct Recovery = 112%  Analysis Date = 09/19/15 
 Pct Recovery = 112%  Analysis Date = 09/19/15 
 Pct Recovery = 112%  Analysis Date = 09/15/15 
 Pct Recovery = 112%  Analysis Date = 09/15/15 
 Pct Recovery = 112%  Analysis Date = 09/11/15 
 Pct Recovery = 111%  Analysis Date = 09/11/15 
 Pct Recovery = 111%  Analysis Date = 09/06/15 
 Pct Recovery = 111%  Analysis Date = 09/06/15 
 Pct Recovery = 111%  Analysis Date = 09/02/15 
 Pct Recovery = 110%  Analysis Date = 09/02/15 
 Pct Recovery = 110%  Analysis Date = 08/29/15 
 Pct Recovery = 110%  Analysis Date = 08/29/15 
 Pct Recovery = 110%  Analysis Date = 08/25/15 
 Pct Recovery = 109%  Analysis Date = 08/25/15 
 Pct Recovery = 109%  Analysis Date = 08/21/15 
 Pct Recovery = 108%  Analysis Date = 08/21/15 
 Pct Recovery = 108%  Analysis Date = 08/17/15 
 Pct Recovery = 108%  Analysis Date = 08/17/15 
 Pct Recovery = 108%  Analysis Date = 08/13/15 
 Pct Recovery = 107%  Analysis Date = 08/13/15 
 Pct Recovery = 107%  Analysis Date = 08/08/15 
 Pct Recovery = 106%  Analysis Date = 08/08/15 
 Pct Recovery = 106%  Analysis Date = 08/04/15 
 Pct Recovery = 105%  Analysis Date = 08/04/15 
 Pct Recovery = 105%  Analysis Date = 07/31/15 
 Pct Recovery = 104%  Analysis Date = 07/31/15 
 Pct Recovery = 104%  Analysis Date = 07/27/15 
 Pct Recovery = 103%  Analysis Date = 07/27/15 
 Pct Recovery = 103%  Analysis Date = 07/23/15 
 Pct Recovery = 102%  Analysis Date = 07/23/15 
 Pct Recovery = 102%  Analysis Date = 07/19/15 
 Pct Recovery = 102%  Analysis Date = 07/19/15 
 Pct Recovery = 102%  Analysis Date = 07/15/15 
 Pct Recovery = 101%  Analysis Date = 07/15/15 
 Pct Recovery = 101%  Analysis Date = 07/11/15 
 Pct Recovery = 100%  Analysis Date = 07/11/15 
 Pct Recovery = 100%  Analysis Date = 07/06/15 
 Pct Recovery = 99%  Analysis Date = 07/06/15 
 Pct Recovery = 99%  Analysis Date = 07/02/15 
 Pct Recovery = 98%  Analysis Date = 07/02/15 
 Pct Recovery = 98%  Analysis Date = 06/28/15 
 Pct Recovery = 97%  Analysis Date = 06/28/15 
 Pct Recovery = 97%  Analysis Date = 06/24/15 
 Pct Recovery = 96%  Analysis Date = 06/24/15 
 Pct Recovery = 96%  Analysis Date = 06/20/15 
 Pct Recovery = 95%  Analysis Date = 06/20/15 
 Pct Recovery = 95%  Analysis Date = 06/16/15 
 Pct Recovery = 95%  Analysis Date = 06/16/15 
 Pct Recovery = 95%  Analysis Date = 06/12/15 
 Pct Recovery = 94%  Analysis Date = 06/12/15 
 Pct Recovery = 94%  Analysis Date = 06/07/15 
 Pct Recovery = 93%  Analysis Date = 06/07/15 
 Pct Recovery = 93%  Analysis Date = 06/03/15 
 Pct Recovery = 92%  Analysis Date = 06/03/15 
 Pct Recovery = 92%  Analysis Date = 05/30/15 
 Pct Recovery = 91%  Analysis Date = 05/30/15 
 Pct Recovery = 91%  Analysis Date = 05/26/15 
 Pct Recovery = 90%  Analysis Date = 05/26/15 
 Pct Recovery = 90%  Analysis Date = 05/22/15 
 Pct Recovery = 89%  Analysis Date = 05/22/15 
 Pct Recovery = 89%  Analysis Date = 05/18/15 
 Pct Recovery = 88%  Analysis Date = 05/18/15 
 Pct Recovery = 88%  Analysis Date = 05/14/15 
 Pct Recovery = 87%  Analysis Date = 05/14/15 
 Pct Recovery = 87%  Analysis Date = 05/10/15 
 Pct Recovery = 86%  Analysis Date = 05/10/15 
 Pct Recovery = 86%  Analysis Date = 05/05/15 
 Pct Recovery = 85%  Analysis Date = 05/05/15 
 Pct Recovery = 85%  Analysis Date = 05/01/15 
 Pct Recovery = 85%  Analysis Date = 05/01/15 
 Pct Recovery = 85%  Analysis Date = 04/27/15 
 Pct Recovery = 84%  Analysis Date = 04/27/15 
 Pct Recovery = 84%  Analysis Date = 04/23/15 
 Pct Recovery = 83%  Analysis Date = 04/23/15 
 Pct Recovery = 83%  Analysis Date = 04/19/15 
 Pct Recovery = 83%  Analysis Date = 04/19/15 
 Pct Recovery = 83%  Analysis Date = 04/15/15 
 Pct Recovery = 82%  Analysis Date = 04/15/15 
 Pct Recovery = 82%  Analysis Date = 04/11/15 
 Pct Recovery = 81%  Analysis Date = 04/11/15 
 Pct Recovery = 81%  Analysis Date = 04/06/15 
 Pct Recovery = 80%  Analysis Date = 04/06/15 
 Pct Recovery = 80%  Analysis Date = 04/02/15 
 Pct Recovery = 80%  Analysis Date = 04/02/15 
 Pct Recovery = 80%  Analysis Date = 03/29/15 
 Pct Recovery = 79%  Analysis Date = 03/29/15 
 Pct Recovery = 79%  Analysis Date = 03/25/15 
 Pct Recovery = 78%  Analysis Date = 03/25/15 
 Pct Recovery = 78%  Analysis Date = 03/21/15 
 Pct Recovery = 78%  Analysis Date = 03/21/15 
 Pct Recovery = 78%  Analysis Date = 03/17/15 
 Pct Recovery = 77%  Analysis Date = 03/17/15 
 Pct Recovery = 77%  Analysis Date = 03/13/15 
 Pct Recovery = 76%  Analysis Date = 03/13/15 
 Pct Recovery = 76%  Analysis Date = 03/08/15 
 Pct Recovery = 75%  Analysis Date = 03/08/15 
 Pct Recovery = 75%  Analysis Date = 03/04/15 
 Pct Recovery = 75%  Analysis Date = 03/04/15 
 Pct Recovery = 75%  Analysis Date = 02/28/15 
 Pct Recovery = 74%  Analysis Date = 02/28/15 
 Pct Recovery = 74%  Analysis Date = 02/24/15 
 Pct Recovery = 73%  Analysis Date = 02/24/15 
 Pct Recovery = 73%  Analysis Date = 02/20/15 
 Pct Recovery = 72%  Analysis Date = 02/20/15 
 Pct Recovery = 72%  Analysis Date = 02/16/15 
 Pct Recovery = 72%  Analysis Date = 02/16/15 
 Pct Recovery = 72%  Analysis Date = 02/12/15 
 Pct Recovery = 71%  Analysis Date = 02/12/15 
 Pct Recovery = 71%  Analysis Date = 02/08/15 
 Pct Recovery = 70%  Analysis Date = 02/08/15 
 Pct Recovery = 70%  Analysis Date = 02/03/15 
 Pct Recovery = 70%  Analysis Date = 02/03/15 
 Pct Recovery = 70%  Analysis Date = 01/30/15 
 Pct Recovery = 69%  Analysis Date = 01/30/15 
 Pct Recovery = 69%  Analysis Date = 01/26/15 
 Pct Recovery = 68%  Analysis Date = 01/26/15 
 Pct Recovery = 68%  Analysis Date = 01/22/15 
 Pct Recovery = 67%  Analysis Date = 01/22/15 
 Pct Recovery = 67%  Analysis Date = 01/18/15 
 Pct Recovery = 67%  Analysis Date = 01/18/15 
 Pct Recovery = 67%  Analysis Date = 01/14/15 
 Pct Recovery = 66%  Analysis Date = 01/14/15 
 Pct Recovery = 66%  Analysis Date = 01/10/15 
 Pct Recovery = 65%  Analysis Date = 01/10/15 
 Pct Recovery = 65%  Analysis Date = 01/05/15 
 Pct Recovery = 65%  Analysis Date = 01/05/15 
 Pct Recovery = 65%  Analysis Date = 01/01/15 
 Pct Recovery = 64%  Analysis Date = 01/01/15 
 Pct Recovery = 64%  Analysis Date = 12/28/14 
 Pct Recovery = 64%  Analysis Date = 12/28/14 
 Pct Recovery = 64%  Analysis Date = 12/24/14 
 Pct Recovery = 63%  Analysis Date = 12/24/14 
 Pct Recovery = 63%  Analysis Date = 12/20/14 
 Pct Recovery = 63%  Analysis Date = 12/20/14 
 Pct Recovery = 63%  Analysis Date = 12/16/14 
 Pct Recovery = 62%  Analysis Date = 12/16/14 
 Pct Recovery = 62%  Analysis Date = 12/12/14 
 Pct Recovery = 62%  Analysis Date = 12/12/14 
 Pct Recovery = 62%  Analysis Date = 12/08/14 
 Pct Recovery = 61%  Analysis Date = 12/08/14 
 Pct Recovery = 61%  Analysis Date = 12/03/14 
 Pct Recovery = 61%  Analysis Date = 12/03/14 
 Pct Recovery = 61%  Analysis Date = 11/29/14 
 Pct Recovery = 60%  Analysis Date = 11/29/14 
 Pct Recovery = 60%  Analysis Date = 11/25/14 
 Pct Recovery = 60%  Analysis Date = 11/25/14 
 Pct Recovery = 60%  Analysis Date = 11/21/14 
 Pct Recovery = 59%  Analysis Date = 11/21/14 
 Pct Recovery = 59%  Analysis Date = 11/17/14 
 Pct Recovery = 59%  Analysis Date = 11/17/14 
 Pct Recovery = 59%  Analysis Date = 11/13/14 
 Pct Recovery = 58%  Analysis Date = 11/13/14 
 Pct Recovery = 58%  Analysis Date = 11/09/14 
 Pct Recovery = 58%  Analysis Date = 11/09/14 
 Pct Recovery = 58%  Analysis Date = 11/04/14 
 Pct Recovery = 57%  Analysis Date = 11/04/14 
 Pct Recovery = 57%  Analysis Date = 10/31/14 
 Pct Recovery = 57%  Analysis Date = 10/31/14 
 Pct Recovery = 57%  Analysis Date = 10/27/14 
 Pct Recovery = 56%  Analysis Date = 10/27/14 
 Pct Recovery = 56%  Analysis Date = 10/23/14 
 Pct Recovery = 56%  Analysis Date = 10/23/14 
 Pct Recovery = 56%  Analysis Date = 10/19/14 
 Pct Recovery = 55%  Analysis Date = 10/19/14 
 Pct Recovery = 55%  Analysis Date = 10/15/14 
 Pct Recovery = 55%  Analysis Date = 10/15/14 
 Pct Recovery = 55%  Analysis Date = 10/11/14 
 Pct Recovery = 55%  Analysis Date = 10/11/14 
 Pct Recovery = 55%  Analysis Date = 10/06/14 
 Pct Recovery = 54%  Analysis Date = 10/06/14 
 Pct Recovery = 54%  Analysis Date = 10/02/14 
 Pct Recovery = 54%  Analysis Date = 10/02/14 
 Pct Recovery = 54%  Analysis Date = 09/28/14 
 Pct Recovery = 53%  Analysis Date = 09/28/14 
 Pct Recovery = 53%  Analysis Date = 09/24/14 
 Pct Recovery = 53%  Analysis Date = 09/24/14 
 Pct Recovery = 53%  Analysis Date = 09/20/14 
 Pct Recovery = 52%  Analysis Date = 09/20/14 
 Pct Recovery = 52%  Analysis Date = 09/16/14 
 Pct Recovery = 52%  Analysis Date = 09/16/14 
 Pct Recovery = 52%  Analysis Date = 09/12/14 
 Pct Recovery = 51%  Analysis Date = 09/12/14 
 Pct Recovery = 51%  Analysis Date = 09/08/14 
 Pct Recovery = 51%  Analysis Date = 09/08/14 
 Pct Recovery = 51%  Analysis Date = 09/03/14 
 Pct Recovery = 50%  Analysis Date = 09/03/14 
 Pct Recovery = 50%  Analysis Date = 08/30/14 
 Pct Recovery = 50%  Analysis Date = 08/30/14 
 Pct Recovery = 50%  Analysis Date = 08/26/14 
 Pct Recovery = 49%  Analysis Date = 08/26/14 
 Pct Recovery = 49%  Analysis Date = 08/22/14 
 Pct Recovery = 49%  Analysis Date = 08/22/14 
 Pct Recovery = 49%  Analysis Date = 08/18/14 
 Pct Recovery = 48%  Analysis Date = 08/18/14 
 Pct Recovery = 48%  Analysis Date = 08/14/14 
 Pct Recovery = 48%  Analysis Date = 08/14/14 
 Pct Recovery = 48%  Analysis Date = 08/10/14 
 Pct Recovery = 47%  Analysis Date = 08/10/14 
 Pct Recovery = 47%  Analysis Date = 08/05/14 
 Pct Recovery = 47%  Analysis Date = 08/05/14 
 Pct Recovery = 47%  Analysis Date = 08/01/14 
 Pct Recovery = 46%  Analysis Date = 08/01/14 
 Pct Recovery = 46%  Analysis Date = 07/28/14 
 Pct Recovery = 46%  Analysis Date = 07/28/14 
 Pct Recovery = 46%  Analysis Date = 07/24/14 
 Pct Recovery = 45%  Analysis Date = 07/24/14 
 Pct Recovery = 45%  Analysis Date = 07/20/14 
 Pct Recovery = 45%  Analysis Date = 07/20/14 
 Pct Recovery = 45%  Analysis Date = 07/16/14 
 Pct Recovery = 45%  Analysis Date = 07/16/14 
 Pct Recovery = 45%  Analysis Date = 07/12/14 
 Pct Recovery = 44%  Analysis Date = 07/12/14 
 Pct Recovery = 44%  Analysis Date = 07/08/14 
 Pct Recovery = 44%  Analysis Date = 07/08/14 
 Pct Recovery = 44%  Analysis Date = 07/03/14 
 Pct Recovery = 43%  Analysis Date = 07/03/14 
 Pct Recovery = 43%  Analysis Date = 06/29/14 
 Pct Recovery = 43%  Analysis Date = 06/29/14 
 Pct Recovery = 43%  Analysis Date = 06/25/14 
 Pct Recovery = 42%  Analysis Date = 06/25/14 
 Pct Recovery = 42%  Analysis Date = 06/21/14 
 Pct Recovery = 42%  Analysis Date = 06/21/14 
 Pct Recovery = 42%  Analysis Date = 06/17/14 
 Pct Recovery = 41%  Analysis Date = 06/17/14 
 Pct Recovery = 41%  Analysis Date = 06/13/14 
 Pct Recovery = 41%  Analysis Date = 06/13/14 
 Pct Recovery = 41%  Analysis Date = 06/09/14 
 Pct Recovery = 41%  Analysis Date = 06/09/14 
 Pct Recovery = 41%  Analysis Date = 06/04/14 
 Pct Recovery = 40%  Analysis Date = 06/04/14 
 Pct Recovery = 40%  Analysis Date = 05/31/14 
 Pct Recovery = 40%  Analysis Date = 05/31/14 
 Pct Recovery = 40%  Analysis Date = 05/27/14 
 Pct Recovery = 40%  Analysis Date = 05/27/14 
 Pct Recovery = 40%  Analysis Date = 05/23/14 
 Pct Recovery = 39%  Analysis Date = 05/23/14 
 Pct Recovery = 39%  Analysis Date = 05/19/14 
 Pct Recovery = 39%  Analysis Date = 05/19/14 
 Pct Recovery = 39%  Analysis Date = 05/15/14 
 Pct Recovery = 38%  Analysis Date = 05/15/14 
 Pct Recovery = 38%  Analysis Date = 05/11/14 
 Pct Recovery = 38%  Analysis Date = 05/11/14 
 Pct Recovery = 38%  Analysis Date = 05/07/14 
 Pct Recovery = 38%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
METHYL ACETATE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 38 88% 32% 99% 46%
Total 38 88% 32% 99% 46%

Sample Statistics
METHYL ACETATE

Characteristic N % % Basis
Plotted 38 100% Spiked
Estimated Values 8 21% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 38 .  
False Negatives 0 0% 0 out of 38
Not Spiked 17 .  
False Positives 6 35% 6 out of 17

BQS OBSP Determination:
N-PENTANAL
METHOD: 4437 , TESTIDCODE: 77061GM016
Open Data Set

 Analysis Date = 08/11/16 
 SpikeMix = Phenova B20160303: 25 µl & Supelco LC20145V: 25 µl & NSI 041416HVOC: 25 µl 
 Pct Recovery = 83%  Analysis Date = 03/19/15 
 SpikeMix = Supelco LC06437: 20 µl & NSI 031814: 20 µl 
 Pct Recovery = 84%  Analysis Date = 01/10/15 
 SpikeMix = Abs 032014: 20 µl & ERA 0321-14-05A: 20 µl 
 Pct Recovery = 67%  Analysis Date = 08/20/14 
 SpikeMix = Supelco LC06437: 20 µl & Abs 032014: 20 µl 
 Pct Recovery = 70%  Analysis Date = 07/23/14 
 SpikeMix = Accu 214031128: 20 µl & Abs 032014: 20 µl 
 Pct Recovery = 69%  Analysis Date = 07/03/14 
 SpikeMix = Abs 032014: 20 µl & ChemService 2615700: 20 µl 
 Pct Recovery = 74%  Analysis Date = 06/06/14 
 SpikeMix = NSI 031814: 20 µl & ChemService 2615700: 20 µl 
 Pct Recovery = 83%  Analysis Date = 05/07/14 
 SpikeMix = NSI 031814: 20 µl & Accu 214031128: 20 µl 
 Pct Recovery = 70%  Analysis Date = 01/22/16 
 SpikeMix = NSI 050515HVOC: 25 µl & ERA 0601-15-05: 25 µl 
 Pct Recovery = 81%  Analysis Date = 10/09/15 
 SpikeMix = ERA 0601-15-05: 25 µl & Accu 215041338: 25 µl 
 Pct Recovery = 93%  Analysis Date = 07/06/16 
 SpikeMix = Phenova B20160303: 15 µl & Accu 216041354: 15 µl & NSI 041416HVOC: 15 µl 
 Pct Recovery = 97%  Analysis Date = 06/03/16 
 SpikeMix = NSI 041516: 15 µl & Phenova B20160303: 15 µl & NSI 041416HVOC: 15 µl 
 Pct Recovery = 81%  Analysis Date = 09/24/15 
 SpikeMix = Abs 040315: 15 µl & ERA 0601-15-05: 15 µl 
 Pct Recovery = 81%  Analysis Date = 08/24/15 
 SpikeMix = ERA 0601-15-05: 15 µl & Supelco LC13544: 15 µl 
 Pct Recovery = 81%  Analysis Date = 04/25/15 
 SpikeMix = Abs 032014: 10 µl & ERA 0321-14-05A: 10 µl 
 Pct Recovery = 68%  Analysis Date = 12/13/14 
 SpikeMix = Accu 214031128: 10 µl & NSI 031814: 10 µl 
 Pct Recovery = 66%  Analysis Date = 09/11/14 
 SpikeMix = Accu 214031128: 10 µl & Abs 032014: 10 µl 
 Pct Recovery = 72%  Analysis Date = 07/30/14 
 SpikeMix = NSI 031814: 10 µl & ChemService 2615700: 10 µl 
 Pct Recovery = 64%  Analysis Date = 06/17/14 
 SpikeMix = Supelco LC06437: 10 µl & Abs 032014: 10 µl 
 Pct Recovery = 78%  Analysis Date = 02/12/16 
 SpikeMix = ERA 0601-15-05: 10 µl & Accu 215041338: 10 µl 
 Pct Recovery = 95%  Analysis Date = 12/05/15 
 SpikeMix = NSI 050515HVOC: 10 µl & ERA 0601-15-05: 10 µl 
 Pct Recovery = 81%  Analysis Date = 11/14/15 
 SpikeMix = ERA 0601-15-05: 10 µl 
 Pct Recovery = 70%  Analysis Date = 08/14/15 
 SpikeMix = Abs 040315: 10 µl & ERA 0601-15-05: 10 µl 
 Pct Recovery = 97%  Analysis Date = 08/10/16 
 Pct Recovery = 88%  Analysis Date = 08/06/16 
 Pct Recovery = 88%  Analysis Date = 08/06/16 
 Pct Recovery = 88%  Analysis Date = 08/02/16 
 Pct Recovery = 88%  Analysis Date = 08/02/16 
 Pct Recovery = 88%  Analysis Date = 07/29/16 
 Pct Recovery = 88%  Analysis Date = 07/29/16 
 Pct Recovery = 88%  Analysis Date = 07/25/16 
 Pct Recovery = 87%  Analysis Date = 07/25/16 
 Pct Recovery = 87%  Analysis Date = 07/21/16 
 Pct Recovery = 87%  Analysis Date = 07/21/16 
 Pct Recovery = 87%  Analysis Date = 07/17/16 
 Pct Recovery = 87%  Analysis Date = 07/17/16 
 Pct Recovery = 87%  Analysis Date = 07/13/16 
 Pct Recovery = 87%  Analysis Date = 07/13/16 
 Pct Recovery = 87%  Analysis Date = 07/08/16 
 Pct Recovery = 87%  Analysis Date = 07/08/16 
 Pct Recovery = 87%  Analysis Date = 07/04/16 
 Pct Recovery = 87%  Analysis Date = 07/04/16 
 Pct Recovery = 87%  Analysis Date = 06/30/16 
 Pct Recovery = 87%  Analysis Date = 06/30/16 
 Pct Recovery = 87%  Analysis Date = 06/26/16 
 Pct Recovery = 87%  Analysis Date = 06/26/16 
 Pct Recovery = 87%  Analysis Date = 06/22/16 
 Pct Recovery = 87%  Analysis Date = 06/22/16 
 Pct Recovery = 87%  Analysis Date = 06/18/16 
 Pct Recovery = 87%  Analysis Date = 06/18/16 
 Pct Recovery = 87%  Analysis Date = 06/14/16 
 Pct Recovery = 87%  Analysis Date = 06/14/16 
 Pct Recovery = 87%  Analysis Date = 06/09/16 
 Pct Recovery = 87%  Analysis Date = 06/09/16 
 Pct Recovery = 87%  Analysis Date = 06/05/16 
 Pct Recovery = 87%  Analysis Date = 06/05/16 
 Pct Recovery = 87%  Analysis Date = 06/01/16 
 Pct Recovery = 87%  Analysis Date = 06/01/16 
 Pct Recovery = 87%  Analysis Date = 05/28/16 
 Pct Recovery = 87%  Analysis Date = 05/28/16 
 Pct Recovery = 87%  Analysis Date = 05/24/16 
 Pct Recovery = 87%  Analysis Date = 05/24/16 
 Pct Recovery = 87%  Analysis Date = 05/20/16 
 Pct Recovery = 87%  Analysis Date = 05/20/16 
 Pct Recovery = 87%  Analysis Date = 05/16/16 
 Pct Recovery = 87%  Analysis Date = 05/16/16 
 Pct Recovery = 87%  Analysis Date = 05/12/16 
 Pct Recovery = 86%  Analysis Date = 05/12/16 
 Pct Recovery = 86%  Analysis Date = 05/07/16 
 Pct Recovery = 86%  Analysis Date = 05/07/16 
 Pct Recovery = 86%  Analysis Date = 05/03/16 
 Pct Recovery = 86%  Analysis Date = 05/03/16 
 Pct Recovery = 86%  Analysis Date = 04/29/16 
 Pct Recovery = 86%  Analysis Date = 04/29/16 
 Pct Recovery = 86%  Analysis Date = 04/25/16 
 Pct Recovery = 86%  Analysis Date = 04/25/16 
 Pct Recovery = 86%  Analysis Date = 04/21/16 
 Pct Recovery = 86%  Analysis Date = 04/21/16 
 Pct Recovery = 86%  Analysis Date = 04/17/16 
 Pct Recovery = 86%  Analysis Date = 04/17/16 
 Pct Recovery = 86%  Analysis Date = 04/13/16 
 Pct Recovery = 86%  Analysis Date = 04/13/16 
 Pct Recovery = 86%  Analysis Date = 04/08/16 
 Pct Recovery = 86%  Analysis Date = 04/08/16 
 Pct Recovery = 86%  Analysis Date = 04/04/16 
 Pct Recovery = 86%  Analysis Date = 04/04/16 
 Pct Recovery = 86%  Analysis Date = 03/31/16 
 Pct Recovery = 86%  Analysis Date = 03/31/16 
 Pct Recovery = 86%  Analysis Date = 03/27/16 
 Pct Recovery = 86%  Analysis Date = 03/27/16 
 Pct Recovery = 86%  Analysis Date = 03/23/16 
 Pct Recovery = 86%  Analysis Date = 03/23/16 
 Pct Recovery = 86%  Analysis Date = 03/19/16 
 Pct Recovery = 86%  Analysis Date = 03/19/16 
 Pct Recovery = 86%  Analysis Date = 03/15/16 
 Pct Recovery = 86%  Analysis Date = 03/15/16 
 Pct Recovery = 86%  Analysis Date = 03/11/16 
 Pct Recovery = 86%  Analysis Date = 03/11/16 
 Pct Recovery = 86%  Analysis Date = 03/06/16 
 Pct Recovery = 86%  Analysis Date = 03/06/16 
 Pct Recovery = 86%  Analysis Date = 03/02/16 
 Pct Recovery = 86%  Analysis Date = 03/02/16 
 Pct Recovery = 86%  Analysis Date = 02/27/16 
 Pct Recovery = 86%  Analysis Date = 02/27/16 
 Pct Recovery = 86%  Analysis Date = 02/23/16 
 Pct Recovery = 86%  Analysis Date = 02/23/16 
 Pct Recovery = 86%  Analysis Date = 02/19/16 
 Pct Recovery = 86%  Analysis Date = 02/19/16 
 Pct Recovery = 86%  Analysis Date = 02/15/16 
 Pct Recovery = 85%  Analysis Date = 02/15/16 
 Pct Recovery = 85%  Analysis Date = 02/11/16 
 Pct Recovery = 85%  Analysis Date = 02/11/16 
 Pct Recovery = 85%  Analysis Date = 02/06/16 
 Pct Recovery = 85%  Analysis Date = 02/06/16 
 Pct Recovery = 85%  Analysis Date = 02/02/16 
 Pct Recovery = 85%  Analysis Date = 02/02/16 
 Pct Recovery = 85%  Analysis Date = 01/29/16 
 Pct Recovery = 85%  Analysis Date = 01/29/16 
 Pct Recovery = 85%  Analysis Date = 01/25/16 
 Pct Recovery = 85%  Analysis Date = 01/25/16 
 Pct Recovery = 85%  Analysis Date = 01/21/16 
 Pct Recovery = 85%  Analysis Date = 01/21/16 
 Pct Recovery = 85%  Analysis Date = 01/17/16 
 Pct Recovery = 85%  Analysis Date = 01/17/16 
 Pct Recovery = 85%  Analysis Date = 01/13/16 
 Pct Recovery = 85%  Analysis Date = 01/13/16 
 Pct Recovery = 85%  Analysis Date = 01/08/16 
 Pct Recovery = 85%  Analysis Date = 01/08/16 
 Pct Recovery = 85%  Analysis Date = 01/04/16 
 Pct Recovery = 85%  Analysis Date = 01/04/16 
 Pct Recovery = 85%  Analysis Date = 12/31/15 
 Pct Recovery = 85%  Analysis Date = 12/31/15 
 Pct Recovery = 85%  Analysis Date = 12/27/15 
 Pct Recovery = 85%  Analysis Date = 12/27/15 
 Pct Recovery = 85%  Analysis Date = 12/23/15 
 Pct Recovery = 85%  Analysis Date = 12/23/15 
 Pct Recovery = 85%  Analysis Date = 12/19/15 
 Pct Recovery = 85%  Analysis Date = 12/19/15 
 Pct Recovery = 85%  Analysis Date = 12/15/15 
 Pct Recovery = 85%  Analysis Date = 12/15/15 
 Pct Recovery = 85%  Analysis Date = 12/11/15 
 Pct Recovery = 85%  Analysis Date = 12/11/15 
 Pct Recovery = 85%  Analysis Date = 12/06/15 
 Pct Recovery = 85%  Analysis Date = 12/06/15 
 Pct Recovery = 85%  Analysis Date = 12/02/15 
 Pct Recovery = 85%  Analysis Date = 12/02/15 
 Pct Recovery = 85%  Analysis Date = 11/28/15 
 Pct Recovery = 84%  Analysis Date = 11/28/15 
 Pct Recovery = 84%  Analysis Date = 11/24/15 
 Pct Recovery = 84%  Analysis Date = 11/24/15 
 Pct Recovery = 84%  Analysis Date = 11/20/15 
 Pct Recovery = 84%  Analysis Date = 11/20/15 
 Pct Recovery = 84%  Analysis Date = 11/16/15 
 Pct Recovery = 84%  Analysis Date = 11/16/15 
 Pct Recovery = 84%  Analysis Date = 11/12/15 
 Pct Recovery = 84%  Analysis Date = 11/12/15 
 Pct Recovery = 84%  Analysis Date = 11/07/15 
 Pct Recovery = 84%  Analysis Date = 11/07/15 
 Pct Recovery = 84%  Analysis Date = 11/03/15 
 Pct Recovery = 84%  Analysis Date = 11/03/15 
 Pct Recovery = 84%  Analysis Date = 10/30/15 
 Pct Recovery = 84%  Analysis Date = 10/30/15 
 Pct Recovery = 84%  Analysis Date = 10/26/15 
 Pct Recovery = 84%  Analysis Date = 10/26/15 
 Pct Recovery = 84%  Analysis Date = 10/22/15 
 Pct Recovery = 84%  Analysis Date = 10/22/15 
 Pct Recovery = 84%  Analysis Date = 10/18/15 
 Pct Recovery = 84%  Analysis Date = 10/18/15 
 Pct Recovery = 84%  Analysis Date = 10/14/15 
 Pct Recovery = 84%  Analysis Date = 10/14/15 
 Pct Recovery = 84%  Analysis Date = 10/10/15 
 Pct Recovery = 84%  Analysis Date = 10/10/15 
 Pct Recovery = 84%  Analysis Date = 10/05/15 
 Pct Recovery = 83%  Analysis Date = 10/05/15 
 Pct Recovery = 83%  Analysis Date = 10/01/15 
 Pct Recovery = 83%  Analysis Date = 10/01/15 
 Pct Recovery = 83%  Analysis Date = 09/27/15 
 Pct Recovery = 83%  Analysis Date = 09/27/15 
 Pct Recovery = 83%  Analysis Date = 09/23/15 
 Pct Recovery = 83%  Analysis Date = 09/23/15 
 Pct Recovery = 83%  Analysis Date = 09/19/15 
 Pct Recovery = 83%  Analysis Date = 09/19/15 
 Pct Recovery = 83%  Analysis Date = 09/15/15 
 Pct Recovery = 83%  Analysis Date = 09/15/15 
 Pct Recovery = 83%  Analysis Date = 09/11/15 
 Pct Recovery = 83%  Analysis Date = 09/11/15 
 Pct Recovery = 83%  Analysis Date = 09/06/15 
 Pct Recovery = 83%  Analysis Date = 09/06/15 
 Pct Recovery = 83%  Analysis Date = 09/02/15 
 Pct Recovery = 82%  Analysis Date = 09/02/15 
 Pct Recovery = 82%  Analysis Date = 08/29/15 
 Pct Recovery = 82%  Analysis Date = 08/29/15 
 Pct Recovery = 82%  Analysis Date = 08/25/15 
 Pct Recovery = 82%  Analysis Date = 08/25/15 
 Pct Recovery = 82%  Analysis Date = 08/21/15 
 Pct Recovery = 82%  Analysis Date = 08/21/15 
 Pct Recovery = 82%  Analysis Date = 08/17/15 
 Pct Recovery = 82%  Analysis Date = 08/17/15 
 Pct Recovery = 82%  Analysis Date = 08/13/15 
 Pct Recovery = 82%  Analysis Date = 08/13/15 
 Pct Recovery = 82%  Analysis Date = 08/08/15 
 Pct Recovery = 81%  Analysis Date = 08/08/15 
 Pct Recovery = 81%  Analysis Date = 08/04/15 
 Pct Recovery = 81%  Analysis Date = 08/04/15 
 Pct Recovery = 81%  Analysis Date = 07/31/15 
 Pct Recovery = 81%  Analysis Date = 07/31/15 
 Pct Recovery = 81%  Analysis Date = 07/27/15 
 Pct Recovery = 81%  Analysis Date = 07/27/15 
 Pct Recovery = 81%  Analysis Date = 07/23/15 
 Pct Recovery = 81%  Analysis Date = 07/23/15 
 Pct Recovery = 81%  Analysis Date = 07/19/15 
 Pct Recovery = 81%  Analysis Date = 07/19/15 
 Pct Recovery = 81%  Analysis Date = 07/15/15 
 Pct Recovery = 80%  Analysis Date = 07/15/15 
 Pct Recovery = 80%  Analysis Date = 07/11/15 
 Pct Recovery = 80%  Analysis Date = 07/11/15 
 Pct Recovery = 80%  Analysis Date = 07/06/15 
 Pct Recovery = 80%  Analysis Date = 07/06/15 
 Pct Recovery = 80%  Analysis Date = 07/02/15 
 Pct Recovery = 80%  Analysis Date = 07/02/15 
 Pct Recovery = 80%  Analysis Date = 06/28/15 
 Pct Recovery = 80%  Analysis Date = 06/28/15 
 Pct Recovery = 80%  Analysis Date = 06/24/15 
 Pct Recovery = 79%  Analysis Date = 06/24/15 
 Pct Recovery = 79%  Analysis Date = 06/20/15 
 Pct Recovery = 79%  Analysis Date = 06/20/15 
 Pct Recovery = 79%  Analysis Date = 06/16/15 
 Pct Recovery = 79%  Analysis Date = 06/16/15 
 Pct Recovery = 79%  Analysis Date = 06/12/15 
 Pct Recovery = 79%  Analysis Date = 06/12/15 
 Pct Recovery = 79%  Analysis Date = 06/07/15 
 Pct Recovery = 79%  Analysis Date = 06/07/15 
 Pct Recovery = 79%  Analysis Date = 06/03/15 
 Pct Recovery = 79%  Analysis Date = 06/03/15 
 Pct Recovery = 79%  Analysis Date = 05/30/15 
 Pct Recovery = 78%  Analysis Date = 05/30/15 
 Pct Recovery = 78%  Analysis Date = 05/26/15 
 Pct Recovery = 78%  Analysis Date = 05/26/15 
 Pct Recovery = 78%  Analysis Date = 05/22/15 
 Pct Recovery = 78%  Analysis Date = 05/22/15 
 Pct Recovery = 78%  Analysis Date = 05/18/15 
 Pct Recovery = 78%  Analysis Date = 05/18/15 
 Pct Recovery = 78%  Analysis Date = 05/14/15 
 Pct Recovery = 78%  Analysis Date = 05/14/15 
 Pct Recovery = 78%  Analysis Date = 05/10/15 
 Pct Recovery = 78%  Analysis Date = 05/10/15 
 Pct Recovery = 78%  Analysis Date = 05/05/15 
 Pct Recovery = 77%  Analysis Date = 05/05/15 
 Pct Recovery = 77%  Analysis Date = 05/01/15 
 Pct Recovery = 77%  Analysis Date = 05/01/15 
 Pct Recovery = 77%  Analysis Date = 04/27/15 
 Pct Recovery = 77%  Analysis Date = 04/27/15 
 Pct Recovery = 77%  Analysis Date = 04/23/15 
 Pct Recovery = 77%  Analysis Date = 04/23/15 
 Pct Recovery = 77%  Analysis Date = 04/19/15 
 Pct Recovery = 77%  Analysis Date = 04/19/15 
 Pct Recovery = 77%  Analysis Date = 04/15/15 
 Pct Recovery = 76%  Analysis Date = 04/15/15 
 Pct Recovery = 76%  Analysis Date = 04/11/15 
 Pct Recovery = 76%  Analysis Date = 04/11/15 
 Pct Recovery = 76%  Analysis Date = 04/06/15 
 Pct Recovery = 76%  Analysis Date = 04/06/15 
 Pct Recovery = 76%  Analysis Date = 04/02/15 
 Pct Recovery = 76%  Analysis Date = 04/02/15 
 Pct Recovery = 76%  Analysis Date = 03/29/15 
 Pct Recovery = 75%  Analysis Date = 03/29/15 
 Pct Recovery = 75%  Analysis Date = 03/25/15 
 Pct Recovery = 75%  Analysis Date = 03/25/15 
 Pct Recovery = 75%  Analysis Date = 03/21/15 
 Pct Recovery = 75%  Analysis Date = 03/21/15 
 Pct Recovery = 75%  Analysis Date = 03/17/15 
 Pct Recovery = 75%  Analysis Date = 03/17/15 
 Pct Recovery = 75%  Analysis Date = 03/13/15 
 Pct Recovery = 75%  Analysis Date = 03/13/15 
 Pct Recovery = 75%  Analysis Date = 03/08/15 
 Pct Recovery = 74%  Analysis Date = 03/08/15 
 Pct Recovery = 74%  Analysis Date = 03/04/15 
 Pct Recovery = 74%  Analysis Date = 03/04/15 
 Pct Recovery = 74%  Analysis Date = 02/28/15 
 Pct Recovery = 74%  Analysis Date = 02/28/15 
 Pct Recovery = 74%  Analysis Date = 02/24/15 
 Pct Recovery = 74%  Analysis Date = 02/24/15 
 Pct Recovery = 74%  Analysis Date = 02/20/15 
 Pct Recovery = 74%  Analysis Date = 02/20/15 
 Pct Recovery = 74%  Analysis Date = 02/16/15 
 Pct Recovery = 74%  Analysis Date = 02/16/15 
 Pct Recovery = 74%  Analysis Date = 02/12/15 
 Pct Recovery = 74%  Analysis Date = 02/12/15 
 Pct Recovery = 74%  Analysis Date = 02/08/15 
 Pct Recovery = 73%  Analysis Date = 02/08/15 
 Pct Recovery = 73%  Analysis Date = 02/03/15 
 Pct Recovery = 73%  Analysis Date = 02/03/15 
 Pct Recovery = 73%  Analysis Date = 01/30/15 
 Pct Recovery = 73%  Analysis Date = 01/30/15 
 Pct Recovery = 73%  Analysis Date = 01/26/15 
 Pct Recovery = 73%  Analysis Date = 01/26/15 
 Pct Recovery = 73%  Analysis Date = 01/22/15 
 Pct Recovery = 73%  Analysis Date = 01/22/15 
 Pct Recovery = 73%  Analysis Date = 01/18/15 
 Pct Recovery = 73%  Analysis Date = 01/18/15 
 Pct Recovery = 73%  Analysis Date = 01/14/15 
 Pct Recovery = 72%  Analysis Date = 01/14/15 
 Pct Recovery = 72%  Analysis Date = 01/10/15 
 Pct Recovery = 72%  Analysis Date = 01/10/15 
 Pct Recovery = 72%  Analysis Date = 01/05/15 
 Pct Recovery = 72%  Analysis Date = 01/05/15 
 Pct Recovery = 72%  Analysis Date = 01/01/15 
 Pct Recovery = 72%  Analysis Date = 01/01/15 
 Pct Recovery = 72%  Analysis Date = 12/28/14 
 Pct Recovery = 72%  Analysis Date = 12/28/14 
 Pct Recovery = 72%  Analysis Date = 12/24/14 
 Pct Recovery = 72%  Analysis Date = 12/24/14 
 Pct Recovery = 72%  Analysis Date = 12/20/14 
 Pct Recovery = 72%  Analysis Date = 12/20/14 
 Pct Recovery = 72%  Analysis Date = 12/16/14 
 Pct Recovery = 71%  Analysis Date = 12/16/14 
 Pct Recovery = 71%  Analysis Date = 12/12/14 
 Pct Recovery = 71%  Analysis Date = 12/12/14 
 Pct Recovery = 71%  Analysis Date = 12/08/14 
 Pct Recovery = 71%  Analysis Date = 12/08/14 
 Pct Recovery = 71%  Analysis Date = 12/03/14 
 Pct Recovery = 71%  Analysis Date = 12/03/14 
 Pct Recovery = 71%  Analysis Date = 11/29/14 
 Pct Recovery = 71%  Analysis Date = 11/29/14 
 Pct Recovery = 71%  Analysis Date = 11/25/14 
 Pct Recovery = 71%  Analysis Date = 11/25/14 
 Pct Recovery = 71%  Analysis Date = 11/21/14 
 Pct Recovery = 71%  Analysis Date = 11/21/14 
 Pct Recovery = 71%  Analysis Date = 11/17/14 
 Pct Recovery = 71%  Analysis Date = 11/17/14 
 Pct Recovery = 71%  Analysis Date = 11/13/14 
 Pct Recovery = 71%  Analysis Date = 11/13/14 
 Pct Recovery = 71%  Analysis Date = 11/09/14 
 Pct Recovery = 72%  Analysis Date = 11/09/14 
 Pct Recovery = 72%  Analysis Date = 11/04/14 
 Pct Recovery = 72%  Analysis Date = 11/04/14 
 Pct Recovery = 72%  Analysis Date = 10/31/14 
 Pct Recovery = 72%  Analysis Date = 10/31/14 
 Pct Recovery = 72%  Analysis Date = 10/27/14 
 Pct Recovery = 72%  Analysis Date = 10/27/14 
 Pct Recovery = 72%  Analysis Date = 10/23/14 
 Pct Recovery = 72%  Analysis Date = 10/23/14 
 Pct Recovery = 72%  Analysis Date = 10/19/14 
 Pct Recovery = 72%  Analysis Date = 10/19/14 
 Pct Recovery = 72%  Analysis Date = 10/15/14 
 Pct Recovery = 72%  Analysis Date = 10/15/14 
 Pct Recovery = 72%  Analysis Date = 10/11/14 
 Pct Recovery = 72%  Analysis Date = 10/11/14 
 Pct Recovery = 72%  Analysis Date = 10/06/14 
 Pct Recovery = 72%  Analysis Date = 10/06/14 
 Pct Recovery = 72%  Analysis Date = 10/02/14 
 Pct Recovery = 72%  Analysis Date = 10/02/14 
 Pct Recovery = 72%  Analysis Date = 09/28/14 
 Pct Recovery = 72%  Analysis Date = 09/28/14 
 Pct Recovery = 72%  Analysis Date = 09/24/14 
 Pct Recovery = 72%  Analysis Date = 09/24/14 
 Pct Recovery = 72%  Analysis Date = 09/20/14 
 Pct Recovery = 72%  Analysis Date = 09/20/14 
 Pct Recovery = 72%  Analysis Date = 09/16/14 
 Pct Recovery = 72%  Analysis Date = 09/16/14 
 Pct Recovery = 72%  Analysis Date = 09/12/14 
 Pct Recovery = 72%  Analysis Date = 09/12/14 
 Pct Recovery = 72%  Analysis Date = 09/08/14 
 Pct Recovery = 72%  Analysis Date = 09/08/14 
 Pct Recovery = 72%  Analysis Date = 09/03/14 
 Pct Recovery = 72%  Analysis Date = 09/03/14 
 Pct Recovery = 72%  Analysis Date = 08/30/14 
 Pct Recovery = 72%  Analysis Date = 08/30/14 
 Pct Recovery = 72%  Analysis Date = 08/26/14 
 Pct Recovery = 72%  Analysis Date = 08/26/14 
 Pct Recovery = 72%  Analysis Date = 08/22/14 
 Pct Recovery = 72%  Analysis Date = 08/22/14 
 Pct Recovery = 72%  Analysis Date = 08/18/14 
 Pct Recovery = 72%  Analysis Date = 08/18/14 
 Pct Recovery = 72%  Analysis Date = 08/14/14 
 Pct Recovery = 72%  Analysis Date = 08/14/14 
 Pct Recovery = 72%  Analysis Date = 08/10/14 
 Pct Recovery = 72%  Analysis Date = 08/10/14 
 Pct Recovery = 72%  Analysis Date = 08/05/14 
 Pct Recovery = 72%  Analysis Date = 08/05/14 
 Pct Recovery = 72%  Analysis Date = 08/01/14 
 Pct Recovery = 72%  Analysis Date = 08/01/14 
 Pct Recovery = 72%  Analysis Date = 07/28/14 
 Pct Recovery = 72%  Analysis Date = 07/28/14 
 Pct Recovery = 72%  Analysis Date = 07/24/14 
 Pct Recovery = 73%  Analysis Date = 07/24/14 
 Pct Recovery = 73%  Analysis Date = 07/20/14 
 Pct Recovery = 73%  Analysis Date = 07/20/14 
 Pct Recovery = 73%  Analysis Date = 07/16/14 
 Pct Recovery = 73%  Analysis Date = 07/16/14 
 Pct Recovery = 73%  Analysis Date = 07/12/14 
 Pct Recovery = 73%  Analysis Date = 07/12/14 
 Pct Recovery = 73%  Analysis Date = 07/08/14 
 Pct Recovery = 73%  Analysis Date = 07/08/14 
 Pct Recovery = 73%  Analysis Date = 07/03/14 
 Pct Recovery = 73%  Analysis Date = 07/03/14 
 Pct Recovery = 73%  Analysis Date = 06/29/14 
 Pct Recovery = 73%  Analysis Date = 06/29/14 
 Pct Recovery = 73%  Analysis Date = 06/25/14 
 Pct Recovery = 73%  Analysis Date = 06/25/14 
 Pct Recovery = 73%  Analysis Date = 06/21/14 
 Pct Recovery = 73%  Analysis Date = 06/21/14 
 Pct Recovery = 73%  Analysis Date = 06/17/14 
 Pct Recovery = 73%  Analysis Date = 06/17/14 
 Pct Recovery = 73%  Analysis Date = 06/13/14 
 Pct Recovery = 73%  Analysis Date = 06/13/14 
 Pct Recovery = 73%  Analysis Date = 06/09/14 
 Pct Recovery = 73%  Analysis Date = 06/09/14 
 Pct Recovery = 73%  Analysis Date = 06/04/14 
 Pct Recovery = 73%  Analysis Date = 06/04/14 
 Pct Recovery = 73%  Analysis Date = 05/31/14 
 Pct Recovery = 73%  Analysis Date = 05/31/14 
 Pct Recovery = 73%  Analysis Date = 05/27/14 
 Pct Recovery = 74%  Analysis Date = 05/27/14 
 Pct Recovery = 74%  Analysis Date = 05/23/14 
 Pct Recovery = 74%  Analysis Date = 05/23/14 
 Pct Recovery = 74%  Analysis Date = 05/19/14 
 Pct Recovery = 74%  Analysis Date = 05/19/14 
 Pct Recovery = 74%  Analysis Date = 05/15/14 
 Pct Recovery = 74%  Analysis Date = 05/15/14 
 Pct Recovery = 74%  Analysis Date = 05/11/14 
 Pct Recovery = 74%  Analysis Date = 05/11/14 
 Pct Recovery = 74%  Analysis Date = 05/07/14 
 Pct Recovery = 74%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
N-PENTANAL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 23 79% 10% 81% 10%
Total 23 79% 10% 81% 10%

Sample Statistics
N-PENTANAL

Characteristic N % % Basis
Plotted 23 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 23 .  
False Negatives 0 0% 0 out of 23
Not Spiked 32 .  
False Positives 0 0% 0 out of 32

BQS OBSP Determination:
NITROBENZENE
METHOD: 4437 , TESTIDCODE: 34447GM016
Open Data Set

 Analysis Date = 06/29/16 
 SpikeMix = NSI 041516: 40 µl & ChemService 5082800: 40 µl 
 Pct Recovery = 103%  Analysis Date = 08/11/16 
 SpikeMix = Phenova B20160303: 25 µl & Supelco LC20145V: 25 µl & NSI 041416HVOC: 25 µl 
 Pct Recovery = 85%  Analysis Date = 07/14/16 
 SpikeMix = NSI 041516: 25 µl & ChemService 5082800: 25 µl & NSI 041416HVOC: 25 µl 
 Pct Recovery = 81%  Analysis Date = 08/13/14 
 SpikeMix = ERA 0321-14-05: 20 µl & Accu 214031128: 20 µl 
 Pct Recovery = 90%  Analysis Date = 07/23/14 
 SpikeMix = Accu 214031128: 20 µl & Abs 032014: 20 µl 
 Pct Recovery = 103%  Analysis Date = 07/11/14 
 SpikeMix = ChemService 2615700: 20 µl & Accu 214031128: 20 µl 
 Pct Recovery = 108%  Analysis Date = 05/07/14 
 SpikeMix = NSI 031814: 20 µl & Accu 214031128: 20 µl 
 Pct Recovery = 100%  Analysis Date = 03/19/15 
 SpikeMix = Supelco LC06437: 20 µl & NSI 031814: 20 µl 
 Pct Recovery = 112%  Analysis Date = 08/20/14 
 SpikeMix = Supelco LC06437: 20 µl & Abs 032014: 20 µl 
 Pct Recovery = 95%  Analysis Date = 06/07/14 
 SpikeMix = ChemService 2615700: 20 µl & Supelco LC06437: 20 µl 
 Pct Recovery = 105%  Analysis Date = 06/26/15 
 SpikeMix = ChemService 3818700: 25 µl & Accu 215041338: 25 µl 
 Pct Recovery = 90%  Analysis Date = 06/25/15 
 SpikeMix = ChemService 3818700: 25 µl & NSI 050515HVOC: 25 µl 
 Pct Recovery = 95%  Analysis Date = 01/22/16 
 SpikeMix = NSI 050515HVOC: 25 µl & ERA 0601-15-05: 25 µl 
 Pct Recovery = 102%  Analysis Date = 10/09/15 
 SpikeMix = ERA 0601-15-05: 25 µl & Accu 215041338: 25 µl 
 Pct Recovery = 102%  Analysis Date = 07/06/16 
 SpikeMix = Phenova B20160303: 15 µl & Accu 216041354: 15 µl & NSI 041416HVOC: 15 µl 
 Pct Recovery = 84%  Analysis Date = 06/03/16 
 SpikeMix = NSI 041516: 15 µl & Phenova B20160303: 15 µl & NSI 041416HVOC: 15 µl 
 Pct Recovery = 90%  Analysis Date = 07/27/16 
 SpikeMix = ChemService 5082800: 15 µl & Supelco LC20145V: 15 µl & Accu 216041225: 15 µl 
 Pct Recovery = 99%  Analysis Date = 06/23/16 
 SpikeMix = . 
 Pct Recovery = 80%  Analysis Date = 04/28/16 
 SpikeMix = ChemService 3818700: 15 µl & Supelco LC13544: 15 µl 
 Pct Recovery = 89%  Analysis Date = 06/16/15 
 SpikeMix = ChemService 3818700: 15 µl & NSI 050515HVOC: 15 µl 
 Pct Recovery = 98%  Analysis Date = 05/14/15 
 SpikeMix = ChemService 3818700: 15 µl & Supelco LC13544: 15 µl 
 Pct Recovery = 107%  Analysis Date = 09/24/15 
 SpikeMix = Abs 040315: 15 µl & ERA 0601-15-05: 15 µl 
 Pct Recovery = 98%  Analysis Date = 08/24/15 
 SpikeMix = ERA 0601-15-05: 15 µl & Supelco LC13544: 15 µl 
 Pct Recovery = 127%  Analysis Date = 12/13/14 
 SpikeMix = Accu 214031128: 10 µl & NSI 031814: 10 µl 
 Pct Recovery = 122%  Analysis Date = 11/13/14 
 SpikeMix = ERA 0321-14-05A: 10 µl & Accu 214031128: 10 µl 
 Pct Recovery = 102%  Analysis Date = 09/11/14 
 SpikeMix = Accu 214031128: 10 µl & Abs 032014: 10 µl 
 Pct Recovery = 116%  Analysis Date = 05/20/14 
 SpikeMix = ChemService 2615700: 10 µl & Accu 214031128: 10 µl 
 Pct Recovery = 135%  Analysis Date = 11/22/14 
 SpikeMix = ChemService 2615700: 10 µl & Supelco LC06437: 10 µl 
 Pct Recovery = 104%  Analysis Date = 09/06/14 
 SpikeMix = ERA 0321-14-05: 10 µl & Supelco LC06437: 10 µl 
 Pct Recovery = 96%  Analysis Date = 06/17/14 
 SpikeMix = Supelco LC06437: 10 µl & Abs 032014: 10 µl 
 Pct Recovery = 96%  Analysis Date = 04/09/16 
 SpikeMix = Abs 040315: 10 µl & ChemService 3818700: 10 µl 
 Pct Recovery = 93%  Analysis Date = 12/10/15 
 SpikeMix = ChemService 3818700: 10 µl & Supelco LC13544: 10 µl 
 Pct Recovery = 117%  Analysis Date = 10/23/15 
 SpikeMix = Abs 040315: 10 µl & ChemService 3818700: 10 µl 
 Pct Recovery = 110%  Analysis Date = 05/20/15 
 SpikeMix = ChemService 3818700: 10 µl & Accu 215041338: 10 µl 
 Pct Recovery = 121%  Analysis Date = 02/12/16 
 SpikeMix = ERA 0601-15-05: 10 µl & Accu 215041338: 10 µl 
 Pct Recovery = 112%  Analysis Date = 12/05/15 
 SpikeMix = NSI 050515HVOC: 10 µl & ERA 0601-15-05: 10 µl 
 Pct Recovery = 115%  Analysis Date = 11/14/15 
 SpikeMix = ERA 0601-15-05: 10 µl 
 Pct Recovery = 105%  Analysis Date = 08/14/15 
 SpikeMix = Abs 040315: 10 µl & ERA 0601-15-05: 10 µl 
 Pct Recovery = 96%  Analysis Date = 08/10/16 
 Pct Recovery = 86%  Analysis Date = 08/06/16 
 Pct Recovery = 86%  Analysis Date = 08/06/16 
 Pct Recovery = 86%  Analysis Date = 08/02/16 
 Pct Recovery = 87%  Analysis Date = 08/02/16 
 Pct Recovery = 87%  Analysis Date = 07/29/16 
 Pct Recovery = 87%  Analysis Date = 07/29/16 
 Pct Recovery = 87%  Analysis Date = 07/25/16 
 Pct Recovery = 87%  Analysis Date = 07/25/16 
 Pct Recovery = 87%  Analysis Date = 07/21/16 
 Pct Recovery = 88%  Analysis Date = 07/21/16 
 Pct Recovery = 88%  Analysis Date = 07/17/16 
 Pct Recovery = 88%  Analysis Date = 07/17/16 
 Pct Recovery = 88%  Analysis Date = 07/13/16 
 Pct Recovery = 88%  Analysis Date = 07/13/16 
 Pct Recovery = 88%  Analysis Date = 07/08/16 
 Pct Recovery = 89%  Analysis Date = 07/08/16 
 Pct Recovery = 89%  Analysis Date = 07/04/16 
 Pct Recovery = 89%  Analysis Date = 07/04/16 
 Pct Recovery = 89%  Analysis Date = 06/30/16 
 Pct Recovery = 90%  Analysis Date = 06/30/16 
 Pct Recovery = 90%  Analysis Date = 06/26/16 
 Pct Recovery = 90%  Analysis Date = 06/26/16 
 Pct Recovery = 90%  Analysis Date = 06/22/16 
 Pct Recovery = 90%  Analysis Date = 06/22/16 
 Pct Recovery = 90%  Analysis Date = 06/18/16 
 Pct Recovery = 91%  Analysis Date = 06/18/16 
 Pct Recovery = 91%  Analysis Date = 06/14/16 
 Pct Recovery = 91%  Analysis Date = 06/14/16 
 Pct Recovery = 91%  Analysis Date = 06/09/16 
 Pct Recovery = 91%  Analysis Date = 06/09/16 
 Pct Recovery = 91%  Analysis Date = 06/05/16 
 Pct Recovery = 92%  Analysis Date = 06/05/16 
 Pct Recovery = 92%  Analysis Date = 06/01/16 
 Pct Recovery = 92%  Analysis Date = 06/01/16 
 Pct Recovery = 92%  Analysis Date = 05/28/16 
 Pct Recovery = 92%  Analysis Date = 05/28/16 
 Pct Recovery = 92%  Analysis Date = 05/24/16 
 Pct Recovery = 93%  Analysis Date = 05/24/16 
 Pct Recovery = 93%  Analysis Date = 05/20/16 
 Pct Recovery = 93%  Analysis Date = 05/20/16 
 Pct Recovery = 93%  Analysis Date = 05/16/16 
 Pct Recovery = 93%  Analysis Date = 05/16/16 
 Pct Recovery = 93%  Analysis Date = 05/12/16 
 Pct Recovery = 94%  Analysis Date = 05/12/16 
 Pct Recovery = 94%  Analysis Date = 05/07/16 
 Pct Recovery = 94%  Analysis Date = 05/07/16 
 Pct Recovery = 94%  Analysis Date = 05/03/16 
 Pct Recovery = 94%  Analysis Date = 05/03/16 
 Pct Recovery = 94%  Analysis Date = 04/29/16 
 Pct Recovery = 95%  Analysis Date = 04/29/16 
 Pct Recovery = 95%  Analysis Date = 04/25/16 
 Pct Recovery = 95%  Analysis Date = 04/25/16 
 Pct Recovery = 95%  Analysis Date = 04/21/16 
 Pct Recovery = 95%  Analysis Date = 04/21/16 
 Pct Recovery = 95%  Analysis Date = 04/17/16 
 Pct Recovery = 96%  Analysis Date = 04/17/16 
 Pct Recovery = 96%  Analysis Date = 04/13/16 
 Pct Recovery = 96%  Analysis Date = 04/13/16 
 Pct Recovery = 96%  Analysis Date = 04/08/16 
 Pct Recovery = 96%  Analysis Date = 04/08/16 
 Pct Recovery = 96%  Analysis Date = 04/04/16 
 Pct Recovery = 97%  Analysis Date = 04/04/16 
 Pct Recovery = 97%  Analysis Date = 03/31/16 
 Pct Recovery = 97%  Analysis Date = 03/31/16 
 Pct Recovery = 97%  Analysis Date = 03/27/16 
 Pct Recovery = 97%  Analysis Date = 03/27/16 
 Pct Recovery = 97%  Analysis Date = 03/23/16 
 Pct Recovery = 98%  Analysis Date = 03/23/16 
 Pct Recovery = 98%  Analysis Date = 03/19/16 
 Pct Recovery = 98%  Analysis Date = 03/19/16 
 Pct Recovery = 98%  Analysis Date = 03/15/16 
 Pct Recovery = 98%  Analysis Date = 03/15/16 
 Pct Recovery = 98%  Analysis Date = 03/11/16 
 Pct Recovery = 99%  Analysis Date = 03/11/16 
 Pct Recovery = 99%  Analysis Date = 03/06/16 
 Pct Recovery = 99%  Analysis Date = 03/06/16 
 Pct Recovery = 99%  Analysis Date = 03/02/16 
 Pct Recovery = 99%  Analysis Date = 03/02/16 
 Pct Recovery = 99%  Analysis Date = 02/27/16 
 Pct Recovery = 100%  Analysis Date = 02/27/16 
 Pct Recovery = 100%  Analysis Date = 02/23/16 
 Pct Recovery = 100%  Analysis Date = 02/23/16 
 Pct Recovery = 100%  Analysis Date = 02/19/16 
 Pct Recovery = 100%  Analysis Date = 02/19/16 
 Pct Recovery = 100%  Analysis Date = 02/15/16 
 Pct Recovery = 101%  Analysis Date = 02/15/16 
 Pct Recovery = 101%  Analysis Date = 02/11/16 
 Pct Recovery = 101%  Analysis Date = 02/11/16 
 Pct Recovery = 101%  Analysis Date = 02/06/16 
 Pct Recovery = 101%  Analysis Date = 02/06/16 
 Pct Recovery = 101%  Analysis Date = 02/02/16 
 Pct Recovery = 102%  Analysis Date = 02/02/16 
 Pct Recovery = 102%  Analysis Date = 01/29/16 
 Pct Recovery = 102%  Analysis Date = 01/29/16 
 Pct Recovery = 102%  Analysis Date = 01/25/16 
 Pct Recovery = 102%  Analysis Date = 01/25/16 
 Pct Recovery = 102%  Analysis Date = 01/21/16 
 Pct Recovery = 103%  Analysis Date = 01/21/16 
 Pct Recovery = 103%  Analysis Date = 01/17/16 
 Pct Recovery = 103%  Analysis Date = 01/17/16 
 Pct Recovery = 103%  Analysis Date = 01/13/16 
 Pct Recovery = 103%  Analysis Date = 01/13/16 
 Pct Recovery = 103%  Analysis Date = 01/08/16 
 Pct Recovery = 103%  Analysis Date = 01/08/16 
 Pct Recovery = 103%  Analysis Date = 01/04/16 
 Pct Recovery = 104%  Analysis Date = 01/04/16 
 Pct Recovery = 104%  Analysis Date = 12/31/15 
 Pct Recovery = 104%  Analysis Date = 12/31/15 
 Pct Recovery = 104%  Analysis Date = 12/27/15 
 Pct Recovery = 104%  Analysis Date = 12/27/15 
 Pct Recovery = 104%  Analysis Date = 12/23/15 
 Pct Recovery = 105%  Analysis Date = 12/23/15 
 Pct Recovery = 105%  Analysis Date = 12/19/15 
 Pct Recovery = 105%  Analysis Date = 12/19/15 
 Pct Recovery = 105%  Analysis Date = 12/15/15 
 Pct Recovery = 105%  Analysis Date = 12/15/15 
 Pct Recovery = 105%  Analysis Date = 12/11/15 
 Pct Recovery = 106%  Analysis Date = 12/11/15 
 Pct Recovery = 106%  Analysis Date = 12/06/15 
 Pct Recovery = 106%  Analysis Date = 12/06/15 
 Pct Recovery = 106%  Analysis Date = 12/02/15 
 Pct Recovery = 106%  Analysis Date = 12/02/15 
 Pct Recovery = 106%  Analysis Date = 11/28/15 
 Pct Recovery = 106%  Analysis Date = 11/28/15 
 Pct Recovery = 106%  Analysis Date = 11/24/15 
 Pct Recovery = 106%  Analysis Date = 11/24/15 
 Pct Recovery = 106%  Analysis Date = 11/20/15 
 Pct Recovery = 106%  Analysis Date = 11/20/15 
 Pct Recovery = 106%  Analysis Date = 11/16/15 
 Pct Recovery = 106%  Analysis Date = 11/16/15 
 Pct Recovery = 106%  Analysis Date = 11/12/15 
 Pct Recovery = 106%  Analysis Date = 11/12/15 
 Pct Recovery = 106%  Analysis Date = 11/07/15 
 Pct Recovery = 106%  Analysis Date = 11/07/15 
 Pct Recovery = 106%  Analysis Date = 11/03/15 
 Pct Recovery = 106%  Analysis Date = 11/03/15 
 Pct Recovery = 106%  Analysis Date = 10/30/15 
 Pct Recovery = 106%  Analysis Date = 10/30/15 
 Pct Recovery = 106%  Analysis Date = 10/26/15 
 Pct Recovery = 106%  Analysis Date = 10/26/15 
 Pct Recovery = 106%  Analysis Date = 10/22/15 
 Pct Recovery = 106%  Analysis Date = 10/22/15 
 Pct Recovery = 106%  Analysis Date = 10/18/15 
 Pct Recovery = 106%  Analysis Date = 10/18/15 
 Pct Recovery = 106%  Analysis Date = 10/14/15 
 Pct Recovery = 106%  Analysis Date = 10/14/15 
 Pct Recovery = 106%  Analysis Date = 10/10/15 
 Pct Recovery = 106%  Analysis Date = 10/10/15 
 Pct Recovery = 106%  Analysis Date = 10/05/15 
 Pct Recovery = 106%  Analysis Date = 10/05/15 
 Pct Recovery = 106%  Analysis Date = 10/01/15 
 Pct Recovery = 106%  Analysis Date = 10/01/15 
 Pct Recovery = 106%  Analysis Date = 09/27/15 
 Pct Recovery = 106%  Analysis Date = 09/27/15 
 Pct Recovery = 106%  Analysis Date = 09/23/15 
 Pct Recovery = 106%  Analysis Date = 09/23/15 
 Pct Recovery = 106%  Analysis Date = 09/19/15 
 Pct Recovery = 106%  Analysis Date = 09/19/15 
 Pct Recovery = 106%  Analysis Date = 09/15/15 
 Pct Recovery = 106%  Analysis Date = 09/15/15 
 Pct Recovery = 106%  Analysis Date = 09/11/15 
 Pct Recovery = 106%  Analysis Date = 09/11/15 
 Pct Recovery = 106%  Analysis Date = 09/06/15 
 Pct Recovery = 106%  Analysis Date = 09/06/15 
 Pct Recovery = 106%  Analysis Date = 09/02/15 
 Pct Recovery = 106%  Analysis Date = 09/02/15 
 Pct Recovery = 106%  Analysis Date = 08/29/15 
 Pct Recovery = 106%  Analysis Date = 08/29/15 
 Pct Recovery = 106%  Analysis Date = 08/25/15 
 Pct Recovery = 106%  Analysis Date = 08/25/15 
 Pct Recovery = 106%  Analysis Date = 08/21/15 
 Pct Recovery = 106%  Analysis Date = 08/21/15 
 Pct Recovery = 106%  Analysis Date = 08/17/15 
 Pct Recovery = 106%  Analysis Date = 08/17/15 
 Pct Recovery = 106%  Analysis Date = 08/13/15 
 Pct Recovery = 106%  Analysis Date = 08/13/15 
 Pct Recovery = 106%  Analysis Date = 08/08/15 
 Pct Recovery = 106%  Analysis Date = 08/08/15 
 Pct Recovery = 106%  Analysis Date = 08/04/15 
 Pct Recovery = 106%  Analysis Date = 08/04/15 
 Pct Recovery = 106%  Analysis Date = 07/31/15 
 Pct Recovery = 106%  Analysis Date = 07/31/15 
 Pct Recovery = 106%  Analysis Date = 07/27/15 
 Pct Recovery = 106%  Analysis Date = 07/27/15 
 Pct Recovery = 106%  Analysis Date = 07/23/15 
 Pct Recovery = 106%  Analysis Date = 07/23/15 
 Pct Recovery = 106%  Analysis Date = 07/19/15 
 Pct Recovery = 106%  Analysis Date = 07/19/15 
 Pct Recovery = 106%  Analysis Date = 07/15/15 
 Pct Recovery = 106%  Analysis Date = 07/15/15 
 Pct Recovery = 106%  Analysis Date = 07/11/15 
 Pct Recovery = 106%  Analysis Date = 07/11/15 
 Pct Recovery = 106%  Analysis Date = 07/06/15 
 Pct Recovery = 106%  Analysis Date = 07/06/15 
 Pct Recovery = 106%  Analysis Date = 07/02/15 
 Pct Recovery = 106%  Analysis Date = 07/02/15 
 Pct Recovery = 106%  Analysis Date = 06/28/15 
 Pct Recovery = 106%  Analysis Date = 06/28/15 
 Pct Recovery = 106%  Analysis Date = 06/24/15 
 Pct Recovery = 106%  Analysis Date = 06/24/15 
 Pct Recovery = 106%  Analysis Date = 06/20/15 
 Pct Recovery = 106%  Analysis Date = 06/20/15 
 Pct Recovery = 106%  Analysis Date = 06/16/15 
 Pct Recovery = 106%  Analysis Date = 06/16/15 
 Pct Recovery = 106%  Analysis Date = 06/12/15 
 Pct Recovery = 106%  Analysis Date = 06/12/15 
 Pct Recovery = 106%  Analysis Date = 06/07/15 
 Pct Recovery = 106%  Analysis Date = 06/07/15 
 Pct Recovery = 106%  Analysis Date = 06/03/15 
 Pct Recovery = 106%  Analysis Date = 06/03/15 
 Pct Recovery = 106%  Analysis Date = 05/30/15 
 Pct Recovery = 106%  Analysis Date = 05/30/15 
 Pct Recovery = 106%  Analysis Date = 05/26/15 
 Pct Recovery = 106%  Analysis Date = 05/26/15 
 Pct Recovery = 106%  Analysis Date = 05/22/15 
 Pct Recovery = 107%  Analysis Date = 05/22/15 
 Pct Recovery = 107%  Analysis Date = 05/18/15 
 Pct Recovery = 107%  Analysis Date = 05/18/15 
 Pct Recovery = 107%  Analysis Date = 05/14/15 
 Pct Recovery = 107%  Analysis Date = 05/14/15 
 Pct Recovery = 107%  Analysis Date = 05/10/15 
 Pct Recovery = 107%  Analysis Date = 05/10/15 
 Pct Recovery = 107%  Analysis Date = 05/05/15 
 Pct Recovery = 107%  Analysis Date = 05/05/15 
 Pct Recovery = 107%  Analysis Date = 05/01/15 
 Pct Recovery = 106%  Analysis Date = 05/01/15 
 Pct Recovery = 106%  Analysis Date = 04/27/15 
 Pct Recovery = 106%  Analysis Date = 04/27/15 
 Pct Recovery = 106%  Analysis Date = 04/23/15 
 Pct Recovery = 106%  Analysis Date = 04/23/15 
 Pct Recovery = 106%  Analysis Date = 04/19/15 
 Pct Recovery = 106%  Analysis Date = 04/19/15 
 Pct Recovery = 106%  Analysis Date = 04/15/15 
 Pct Recovery = 106%  Analysis Date = 04/15/15 
 Pct Recovery = 106%  Analysis Date = 04/11/15 
 Pct Recovery = 106%  Analysis Date = 04/11/15 
 Pct Recovery = 106%  Analysis Date = 04/06/15 
 Pct Recovery = 106%  Analysis Date = 04/06/15 
 Pct Recovery = 106%  Analysis Date = 04/02/15 
 Pct Recovery = 106%  Analysis Date = 04/02/15 
 Pct Recovery = 106%  Analysis Date = 03/29/15 
 Pct Recovery = 106%  Analysis Date = 03/29/15 
 Pct Recovery = 106%  Analysis Date = 03/25/15 
 Pct Recovery = 106%  Analysis Date = 03/25/15 
 Pct Recovery = 106%  Analysis Date = 03/21/15 
 Pct Recovery = 106%  Analysis Date = 03/21/15 
 Pct Recovery = 106%  Analysis Date = 03/17/15 
 Pct Recovery = 106%  Analysis Date = 03/17/15 
 Pct Recovery = 106%  Analysis Date = 03/13/15 
 Pct Recovery = 106%  Analysis Date = 03/13/15 
 Pct Recovery = 106%  Analysis Date = 03/08/15 
 Pct Recovery = 106%  Analysis Date = 03/08/15 
 Pct Recovery = 106%  Analysis Date = 03/04/15 
 Pct Recovery = 106%  Analysis Date = 03/04/15 
 Pct Recovery = 106%  Analysis Date = 02/28/15 
 Pct Recovery = 106%  Analysis Date = 02/28/15 
 Pct Recovery = 106%  Analysis Date = 02/24/15 
 Pct Recovery = 106%  Analysis Date = 02/24/15 
 Pct Recovery = 106%  Analysis Date = 02/20/15 
 Pct Recovery = 106%  Analysis Date = 02/20/15 
 Pct Recovery = 106%  Analysis Date = 02/16/15 
 Pct Recovery = 106%  Analysis Date = 02/16/15 
 Pct Recovery = 106%  Analysis Date = 02/12/15 
 Pct Recovery = 106%  Analysis Date = 02/12/15 
 Pct Recovery = 106%  Analysis Date = 02/08/15 
 Pct Recovery = 106%  Analysis Date = 02/08/15 
 Pct Recovery = 106%  Analysis Date = 02/03/15 
 Pct Recovery = 106%  Analysis Date = 02/03/15 
 Pct Recovery = 106%  Analysis Date = 01/30/15 
 Pct Recovery = 106%  Analysis Date = 01/30/15 
 Pct Recovery = 106%  Analysis Date = 01/26/15 
 Pct Recovery = 106%  Analysis Date = 01/26/15 
 Pct Recovery = 106%  Analysis Date = 01/22/15 
 Pct Recovery = 106%  Analysis Date = 01/22/15 
 Pct Recovery = 106%  Analysis Date = 01/18/15 
 Pct Recovery = 106%  Analysis Date = 01/18/15 
 Pct Recovery = 106%  Analysis Date = 01/14/15 
 Pct Recovery = 106%  Analysis Date = 01/14/15 
 Pct Recovery = 106%  Analysis Date = 01/10/15 
 Pct Recovery = 106%  Analysis Date = 01/10/15 
 Pct Recovery = 106%  Analysis Date = 01/05/15 
 Pct Recovery = 106%  Analysis Date = 01/05/15 
 Pct Recovery = 106%  Analysis Date = 01/01/15 
 Pct Recovery = 106%  Analysis Date = 01/01/15 
 Pct Recovery = 106%  Analysis Date = 12/28/14 
 Pct Recovery = 106%  Analysis Date = 12/28/14 
 Pct Recovery = 106%  Analysis Date = 12/24/14 
 Pct Recovery = 106%  Analysis Date = 12/24/14 
 Pct Recovery = 106%  Analysis Date = 12/20/14 
 Pct Recovery = 106%  Analysis Date = 12/20/14 
 Pct Recovery = 106%  Analysis Date = 12/16/14 
 Pct Recovery = 106%  Analysis Date = 12/16/14 
 Pct Recovery = 106%  Analysis Date = 12/12/14 
 Pct Recovery = 106%  Analysis Date = 12/12/14 
 Pct Recovery = 106%  Analysis Date = 12/08/14 
 Pct Recovery = 106%  Analysis Date = 12/08/14 
 Pct Recovery = 106%  Analysis Date = 12/03/14 
 Pct Recovery = 106%  Analysis Date = 12/03/14 
 Pct Recovery = 106%  Analysis Date = 11/29/14 
 Pct Recovery = 106%  Analysis Date = 11/29/14 
 Pct Recovery = 106%  Analysis Date = 11/25/14 
 Pct Recovery = 106%  Analysis Date = 11/25/14 
 Pct Recovery = 106%  Analysis Date = 11/21/14 
 Pct Recovery = 106%  Analysis Date = 11/21/14 
 Pct Recovery = 106%  Analysis Date = 11/17/14 
 Pct Recovery = 106%  Analysis Date = 11/17/14 
 Pct Recovery = 106%  Analysis Date = 11/13/14 
 Pct Recovery = 106%  Analysis Date = 11/13/14 
 Pct Recovery = 106%  Analysis Date = 11/09/14 
 Pct Recovery = 106%  Analysis Date = 11/09/14 
 Pct Recovery = 106%  Analysis Date = 11/04/14 
 Pct Recovery = 106%  Analysis Date = 11/04/14 
 Pct Recovery = 106%  Analysis Date = 10/31/14 
 Pct Recovery = 106%  Analysis Date = 10/31/14 
 Pct Recovery = 106%  Analysis Date = 10/27/14 
 Pct Recovery = 106%  Analysis Date = 10/27/14 
 Pct Recovery = 106%  Analysis Date = 10/23/14 
 Pct Recovery = 106%  Analysis Date = 10/23/14 
 Pct Recovery = 106%  Analysis Date = 10/19/14 
 Pct Recovery = 106%  Analysis Date = 10/19/14 
 Pct Recovery = 106%  Analysis Date = 10/15/14 
 Pct Recovery = 106%  Analysis Date = 10/15/14 
 Pct Recovery = 106%  Analysis Date = 10/11/14 
 Pct Recovery = 106%  Analysis Date = 10/11/14 
 Pct Recovery = 106%  Analysis Date = 10/06/14 
 Pct Recovery = 106%  Analysis Date = 10/06/14 
 Pct Recovery = 106%  Analysis Date = 10/02/14 
 Pct Recovery = 106%  Analysis Date = 10/02/14 
 Pct Recovery = 106%  Analysis Date = 09/28/14 
 Pct Recovery = 106%  Analysis Date = 09/28/14 
 Pct Recovery = 106%  Analysis Date = 09/24/14 
 Pct Recovery = 106%  Analysis Date = 09/24/14 
 Pct Recovery = 106%  Analysis Date = 09/20/14 
 Pct Recovery = 106%  Analysis Date = 09/20/14 
 Pct Recovery = 106%  Analysis Date = 09/16/14 
 Pct Recovery = 106%  Analysis Date = 09/16/14 
 Pct Recovery = 106%  Analysis Date = 09/12/14 
 Pct Recovery = 106%  Analysis Date = 09/12/14 
 Pct Recovery = 106%  Analysis Date = 09/08/14 
 Pct Recovery = 106%  Analysis Date = 09/08/14 
 Pct Recovery = 106%  Analysis Date = 09/03/14 
 Pct Recovery = 106%  Analysis Date = 09/03/14 
 Pct Recovery = 106%  Analysis Date = 08/30/14 
 Pct Recovery = 106%  Analysis Date = 08/30/14 
 Pct Recovery = 106%  Analysis Date = 08/26/14 
 Pct Recovery = 106%  Analysis Date = 08/26/14 
 Pct Recovery = 106%  Analysis Date = 08/22/14 
 Pct Recovery = 106%  Analysis Date = 08/22/14 
 Pct Recovery = 106%  Analysis Date = 08/18/14 
 Pct Recovery = 106%  Analysis Date = 08/18/14 
 Pct Recovery = 106%  Analysis Date = 08/14/14 
 Pct Recovery = 106%  Analysis Date = 08/14/14 
 Pct Recovery = 106%  Analysis Date = 08/10/14 
 Pct Recovery = 106%  Analysis Date = 08/10/14 
 Pct Recovery = 106%  Analysis Date = 08/05/14 
 Pct Recovery = 106%  Analysis Date = 08/05/14 
 Pct Recovery = 106%  Analysis Date = 08/01/14 
 Pct Recovery = 106%  Analysis Date = 08/01/14 
 Pct Recovery = 106%  Analysis Date = 07/28/14 
 Pct Recovery = 106%  Analysis Date = 07/28/14 
 Pct Recovery = 106%  Analysis Date = 07/24/14 
 Pct Recovery = 105%  Analysis Date = 07/24/14 
 Pct Recovery = 105%  Analysis Date = 07/20/14 
 Pct Recovery = 105%  Analysis Date = 07/20/14 
 Pct Recovery = 105%  Analysis Date = 07/16/14 
 Pct Recovery = 105%  Analysis Date = 07/16/14 
 Pct Recovery = 105%  Analysis Date = 07/12/14 
 Pct Recovery = 105%  Analysis Date = 07/12/14 
 Pct Recovery = 105%  Analysis Date = 07/08/14 
 Pct Recovery = 105%  Analysis Date = 07/08/14 
 Pct Recovery = 105%  Analysis Date = 07/03/14 
 Pct Recovery = 105%  Analysis Date = 07/03/14 
 Pct Recovery = 105%  Analysis Date = 06/29/14 
 Pct Recovery = 105%  Analysis Date = 06/29/14 
 Pct Recovery = 105%  Analysis Date = 06/25/14 
 Pct Recovery = 105%  Analysis Date = 06/25/14 
 Pct Recovery = 105%  Analysis Date = 06/21/14 
 Pct Recovery = 105%  Analysis Date = 06/21/14 
 Pct Recovery = 105%  Analysis Date = 06/17/14 
 Pct Recovery = 105%  Analysis Date = 06/17/14 
 Pct Recovery = 105%  Analysis Date = 06/13/14 
 Pct Recovery = 105%  Analysis Date = 06/13/14 
 Pct Recovery = 105%  Analysis Date = 06/09/14 
 Pct Recovery = 105%  Analysis Date = 06/09/14 
 Pct Recovery = 105%  Analysis Date = 06/04/14 
 Pct Recovery = 105%  Analysis Date = 06/04/14 
 Pct Recovery = 105%  Analysis Date = 05/31/14 
 Pct Recovery = 105%  Analysis Date = 05/31/14 
 Pct Recovery = 105%  Analysis Date = 05/27/14 
 Pct Recovery = 105%  Analysis Date = 05/27/14 
 Pct Recovery = 105%  Analysis Date = 05/23/14 
 Pct Recovery = 105%  Analysis Date = 05/23/14 
 Pct Recovery = 105%  Analysis Date = 05/19/14 
 Pct Recovery = 105%  Analysis Date = 05/19/14 
 Pct Recovery = 105%  Analysis Date = 05/15/14 
 Pct Recovery = 105%  Analysis Date = 05/15/14 
 Pct Recovery = 105%  Analysis Date = 05/11/14 
 Pct Recovery = 105%  Analysis Date = 05/11/14 
 Pct Recovery = 105%  Analysis Date = 05/07/14 
 Pct Recovery = 105%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
NITROBENZENE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 38 102% 13% 102% 11%
Total 38 102% 13% 102% 11%

Sample Statistics
NITROBENZENE

Characteristic N % % Basis
Plotted 38 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 38 .  
False Negatives 0 0% 0 out of 38
Not Spiked 17 .  
False Positives 0 0% 0 out of 17

BQS OBSP Determination:
TERT-BUTYL ALCOHOL
METHOD: 4437 , TESTIDCODE: 77035GM016
Open Data Set

 Analysis Date = 01/10/15 
 SpikeMix = Abs 032014: 20 µl & ERA 0321-14-05A: 20 µl 
 Pct Recovery = 105%  Analysis Date = 08/20/14 
 SpikeMix = Supelco LC06437: 20 µl & Abs 032014: 20 µl 
 Pct Recovery = 104%  Analysis Date = 07/23/14 
 SpikeMix = Accu 214031128: 20 µl & Abs 032014: 20 µl 
 Pct Recovery = 99%  Analysis Date = 07/03/14 
 SpikeMix = Abs 032014: 20 µl & ChemService 2615700: 20 µl 
 Pct Recovery = 96%  Analysis Date = 03/19/15 
 SpikeMix = Supelco LC06437: 20 µl & NSI 031814: 20 µl 
 Pct Recovery = 117%  Analysis Date = 06/06/14 
 SpikeMix = NSI 031814: 20 µl & ChemService 2615700: 20 µl 
 Pct Recovery = 101%  Analysis Date = 05/07/14 
 SpikeMix = NSI 031814: 20 µl & Accu 214031128: 20 µl 
 Pct Recovery = 102%  Analysis Date = 01/22/16 
 SpikeMix = NSI 050515HVOC: 25 µl & ERA 0601-15-05: 25 µl 
 Pct Recovery = 94%  Analysis Date = 10/09/15 
 SpikeMix = Supelco LC13544: 25 µl & NSI 050515HVOC: 25 µl 
 Pct Recovery = 94%  Analysis Date = 06/25/15 
 SpikeMix = ChemService 3818700: 25 µl & NSI 050515HVOC: 25 µl 
 Pct Recovery = 89%  Analysis Date = 08/12/16 
 SpikeMix = Accu 216041354: 15 µl & Abs 060916HVOC: 15 µl 
 Pct Recovery = 102%  Analysis Date = 11/25/15 
 SpikeMix = Accu 215041338: 15 µl & Abs 040315: 15 µl 
 Pct Recovery = 93%  Analysis Date = 09/24/15 
 SpikeMix = Abs 040315: 15 µl & ERA 0601-15-05: 15 µl 
 Pct Recovery = 91%  Analysis Date = 09/05/15 
 SpikeMix = Accu 215041338: 15 µl & NSI 050515HVOC: 15 µl 
 Pct Recovery = 88%  Analysis Date = 07/30/15 
 SpikeMix = Supelco LC13544: 15 µl & NSI 050515HVOC: 15 µl 
 Pct Recovery = 97%  Analysis Date = 06/16/15 
 SpikeMix = ChemService 3818700: 15 µl & NSI 050515HVOC: 15 µl 
 Pct Recovery = 86%  Analysis Date = 04/25/15 
 SpikeMix = Abs 032014: 10 µl & ERA 0321-14-05A: 10 µl 
 Pct Recovery = 113%  Analysis Date = 09/11/14 
 SpikeMix = Accu 214031128: 10 µl & Abs 032014: 10 µl 
 Pct Recovery = 112%  Analysis Date = 06/17/14 
 SpikeMix = Supelco LC06437: 10 µl & Abs 032014: 10 µl 
 Pct Recovery = 115%  Analysis Date = 12/13/14 
 SpikeMix = Accu 214031128: 10 µl & NSI 031814: 10 µl 
 Pct Recovery = 106%  Analysis Date = 07/30/14 
 SpikeMix = NSI 031814: 10 µl & ChemService 2615700: 10 µl 
 Pct Recovery = 101%  Analysis Date = 04/09/16 
 SpikeMix = Abs 040315: 10 µl & ChemService 3818700: 10 µl 
 Pct Recovery = 101%  Analysis Date = 03/22/16 
 SpikeMix = Supelco LC13544: 10 µl & NSI 050515HVOC: 10 µl 
 Pct Recovery = 98%  Analysis Date = 01/05/16 
 SpikeMix = Accu 215041338: 10 µl & Abs 040315: 10 µl 
 Pct Recovery = 98%  Analysis Date = 12/05/15 
 SpikeMix = NSI 050515HVOC: 10 µl & ERA 0601-15-05: 10 µl 
 Pct Recovery = 94%  Analysis Date = 10/23/15 
 SpikeMix = Abs 040315: 10 µl & ChemService 3818700: 10 µl 
 Pct Recovery = 100%  Analysis Date = 08/14/15 
 SpikeMix = Abs 040315: 10 µl & ERA 0601-15-05: 10 µl 
 Pct Recovery = 97%  Analysis Date = 05/05/15 
 SpikeMix = Supelco LC13544: 10 µl & Abs 040315: 10 µl 
 Pct Recovery = 143%  Analysis Date = 08/11/16 
 Pct Recovery = 102%  Analysis Date = 08/07/16 
 Pct Recovery = 102%  Analysis Date = 08/07/16 
 Pct Recovery = 102%  Analysis Date = 08/03/16 
 Pct Recovery = 102%  Analysis Date = 08/03/16 
 Pct Recovery = 102%  Analysis Date = 07/30/16 
 Pct Recovery = 102%  Analysis Date = 07/30/16 
 Pct Recovery = 102%  Analysis Date = 07/26/16 
 Pct Recovery = 102%  Analysis Date = 07/26/16 
 Pct Recovery = 102%  Analysis Date = 07/22/16 
 Pct Recovery = 102%  Analysis Date = 07/22/16 
 Pct Recovery = 102%  Analysis Date = 07/18/16 
 Pct Recovery = 101%  Analysis Date = 07/18/16 
 Pct Recovery = 101%  Analysis Date = 07/14/16 
 Pct Recovery = 101%  Analysis Date = 07/14/16 
 Pct Recovery = 101%  Analysis Date = 07/09/16 
 Pct Recovery = 101%  Analysis Date = 07/09/16 
 Pct Recovery = 101%  Analysis Date = 07/05/16 
 Pct Recovery = 101%  Analysis Date = 07/05/16 
 Pct Recovery = 101%  Analysis Date = 07/01/16 
 Pct Recovery = 101%  Analysis Date = 07/01/16 
 Pct Recovery = 101%  Analysis Date = 06/27/16 
 Pct Recovery = 101%  Analysis Date = 06/27/16 
 Pct Recovery = 101%  Analysis Date = 06/23/16 
 Pct Recovery = 101%  Analysis Date = 06/23/16 
 Pct Recovery = 101%  Analysis Date = 06/19/16 
 Pct Recovery = 101%  Analysis Date = 06/19/16 
 Pct Recovery = 101%  Analysis Date = 06/15/16 
 Pct Recovery = 101%  Analysis Date = 06/15/16 
 Pct Recovery = 101%  Analysis Date = 06/10/16 
 Pct Recovery = 100%  Analysis Date = 06/10/16 
 Pct Recovery = 100%  Analysis Date = 06/06/16 
 Pct Recovery = 100%  Analysis Date = 06/06/16 
 Pct Recovery = 100%  Analysis Date = 06/02/16 
 Pct Recovery = 100%  Analysis Date = 06/02/16 
 Pct Recovery = 100%  Analysis Date = 05/29/16 
 Pct Recovery = 100%  Analysis Date = 05/29/16 
 Pct Recovery = 100%  Analysis Date = 05/25/16 
 Pct Recovery = 100%  Analysis Date = 05/25/16 
 Pct Recovery = 100%  Analysis Date = 05/21/16 
 Pct Recovery = 100%  Analysis Date = 05/21/16 
 Pct Recovery = 100%  Analysis Date = 05/17/16 
 Pct Recovery = 100%  Analysis Date = 05/17/16 
 Pct Recovery = 100%  Analysis Date = 05/12/16 
 Pct Recovery = 100%  Analysis Date = 05/12/16 
 Pct Recovery = 100%  Analysis Date = 05/08/16 
 Pct Recovery = 100%  Analysis Date = 05/08/16 
 Pct Recovery = 100%  Analysis Date = 05/04/16 
 Pct Recovery = 99%  Analysis Date = 05/04/16 
 Pct Recovery = 99%  Analysis Date = 04/30/16 
 Pct Recovery = 99%  Analysis Date = 04/30/16 
 Pct Recovery = 99%  Analysis Date = 04/26/16 
 Pct Recovery = 99%  Analysis Date = 04/26/16 
 Pct Recovery = 99%  Analysis Date = 04/22/16 
 Pct Recovery = 99%  Analysis Date = 04/22/16 
 Pct Recovery = 99%  Analysis Date = 04/18/16 
 Pct Recovery = 99%  Analysis Date = 04/18/16 
 Pct Recovery = 99%  Analysis Date = 04/13/16 
 Pct Recovery = 99%  Analysis Date = 04/13/16 
 Pct Recovery = 99%  Analysis Date = 04/09/16 
 Pct Recovery = 99%  Analysis Date = 04/09/16 
 Pct Recovery = 99%  Analysis Date = 04/05/16 
 Pct Recovery = 99%  Analysis Date = 04/05/16 
 Pct Recovery = 99%  Analysis Date = 04/01/16 
 Pct Recovery = 99%  Analysis Date = 04/01/16 
 Pct Recovery = 99%  Analysis Date = 03/28/16 
 Pct Recovery = 98%  Analysis Date = 03/28/16 
 Pct Recovery = 98%  Analysis Date = 03/24/16 
 Pct Recovery = 98%  Analysis Date = 03/24/16 
 Pct Recovery = 98%  Analysis Date = 03/20/16 
 Pct Recovery = 98%  Analysis Date = 03/20/16 
 Pct Recovery = 98%  Analysis Date = 03/15/16 
 Pct Recovery = 98%  Analysis Date = 03/15/16 
 Pct Recovery = 98%  Analysis Date = 03/11/16 
 Pct Recovery = 98%  Analysis Date = 03/11/16 
 Pct Recovery = 98%  Analysis Date = 03/07/16 
 Pct Recovery = 98%  Analysis Date = 03/07/16 
 Pct Recovery = 98%  Analysis Date = 03/03/16 
 Pct Recovery = 98%  Analysis Date = 03/03/16 
 Pct Recovery = 98%  Analysis Date = 02/28/16 
 Pct Recovery = 98%  Analysis Date = 02/28/16 
 Pct Recovery = 98%  Analysis Date = 02/24/16 
 Pct Recovery = 98%  Analysis Date = 02/24/16 
 Pct Recovery = 98%  Analysis Date = 02/20/16 
 Pct Recovery = 97%  Analysis Date = 02/20/16 
 Pct Recovery = 97%  Analysis Date = 02/15/16 
 Pct Recovery = 97%  Analysis Date = 02/15/16 
 Pct Recovery = 97%  Analysis Date = 02/11/16 
 Pct Recovery = 97%  Analysis Date = 02/11/16 
 Pct Recovery = 97%  Analysis Date = 02/07/16 
 Pct Recovery = 97%  Analysis Date = 02/07/16 
 Pct Recovery = 97%  Analysis Date = 02/03/16 
 Pct Recovery = 97%  Analysis Date = 02/03/16 
 Pct Recovery = 97%  Analysis Date = 01/30/16 
 Pct Recovery = 97%  Analysis Date = 01/30/16 
 Pct Recovery = 97%  Analysis Date = 01/26/16 
 Pct Recovery = 97%  Analysis Date = 01/26/16 
 Pct Recovery = 97%  Analysis Date = 01/22/16 
 Pct Recovery = 97%  Analysis Date = 01/22/16 
 Pct Recovery = 97%  Analysis Date = 01/17/16 
 Pct Recovery = 97%  Analysis Date = 01/17/16 
 Pct Recovery = 97%  Analysis Date = 01/13/16 
 Pct Recovery = 97%  Analysis Date = 01/13/16 
 Pct Recovery = 97%  Analysis Date = 01/09/16 
 Pct Recovery = 96%  Analysis Date = 01/09/16 
 Pct Recovery = 96%  Analysis Date = 01/05/16 
 Pct Recovery = 96%  Analysis Date = 01/05/16 
 Pct Recovery = 96%  Analysis Date = 01/01/16 
 Pct Recovery = 96%  Analysis Date = 01/01/16 
 Pct Recovery = 96%  Analysis Date = 12/28/15 
 Pct Recovery = 96%  Analysis Date = 12/28/15 
 Pct Recovery = 96%  Analysis Date = 12/24/15 
 Pct Recovery = 96%  Analysis Date = 12/24/15 
 Pct Recovery = 96%  Analysis Date = 12/20/15 
 Pct Recovery = 96%  Analysis Date = 12/20/15 
 Pct Recovery = 96%  Analysis Date = 12/15/15 
 Pct Recovery = 96%  Analysis Date = 12/15/15 
 Pct Recovery = 96%  Analysis Date = 12/11/15 
 Pct Recovery = 96%  Analysis Date = 12/11/15 
 Pct Recovery = 96%  Analysis Date = 12/07/15 
 Pct Recovery = 95%  Analysis Date = 12/07/15 
 Pct Recovery = 95%  Analysis Date = 12/03/15 
 Pct Recovery = 95%  Analysis Date = 12/03/15 
 Pct Recovery = 95%  Analysis Date = 11/29/15 
 Pct Recovery = 95%  Analysis Date = 11/29/15 
 Pct Recovery = 95%  Analysis Date = 11/25/15 
 Pct Recovery = 95%  Analysis Date = 11/25/15 
 Pct Recovery = 95%  Analysis Date = 11/21/15 
 Pct Recovery = 95%  Analysis Date = 11/21/15 
 Pct Recovery = 95%  Analysis Date = 11/16/15 
 Pct Recovery = 95%  Analysis Date = 11/16/15 
 Pct Recovery = 95%  Analysis Date = 11/12/15 
 Pct Recovery = 95%  Analysis Date = 11/12/15 
 Pct Recovery = 95%  Analysis Date = 11/08/15 
 Pct Recovery = 95%  Analysis Date = 11/08/15 
 Pct Recovery = 95%  Analysis Date = 11/04/15 
 Pct Recovery = 95%  Analysis Date = 11/04/15 
 Pct Recovery = 95%  Analysis Date = 10/31/15 
 Pct Recovery = 94%  Analysis Date = 10/31/15 
 Pct Recovery = 94%  Analysis Date = 10/27/15 
 Pct Recovery = 94%  Analysis Date = 10/27/15 
 Pct Recovery = 94%  Analysis Date = 10/23/15 
 Pct Recovery = 94%  Analysis Date = 10/23/15 
 Pct Recovery = 94%  Analysis Date = 10/18/15 
 Pct Recovery = 94%  Analysis Date = 10/18/15 
 Pct Recovery = 94%  Analysis Date = 10/14/15 
 Pct Recovery = 95%  Analysis Date = 10/14/15 
 Pct Recovery = 95%  Analysis Date = 10/10/15 
 Pct Recovery = 95%  Analysis Date = 10/10/15 
 Pct Recovery = 95%  Analysis Date = 10/06/15 
 Pct Recovery = 95%  Analysis Date = 10/06/15 
 Pct Recovery = 95%  Analysis Date = 10/02/15 
 Pct Recovery = 95%  Analysis Date = 10/02/15 
 Pct Recovery = 95%  Analysis Date = 09/28/15 
 Pct Recovery = 95%  Analysis Date = 09/28/15 
 Pct Recovery = 95%  Analysis Date = 09/24/15 
 Pct Recovery = 95%  Analysis Date = 09/24/15 
 Pct Recovery = 95%  Analysis Date = 09/19/15 
 Pct Recovery = 96%  Analysis Date = 09/19/15 
 Pct Recovery = 96%  Analysis Date = 09/15/15 
 Pct Recovery = 96%  Analysis Date = 09/15/15 
 Pct Recovery = 96%  Analysis Date = 09/11/15 
 Pct Recovery = 96%  Analysis Date = 09/11/15 
 Pct Recovery = 96%  Analysis Date = 09/07/15 
 Pct Recovery = 96%  Analysis Date = 09/07/15 
 Pct Recovery = 96%  Analysis Date = 09/03/15 
 Pct Recovery = 96%  Analysis Date = 09/03/15 
 Pct Recovery = 96%  Analysis Date = 08/30/15 
 Pct Recovery = 97%  Analysis Date = 08/30/15 
 Pct Recovery = 97%  Analysis Date = 08/26/15 
 Pct Recovery = 97%  Analysis Date = 08/26/15 
 Pct Recovery = 97%  Analysis Date = 08/21/15 
 Pct Recovery = 98%  Analysis Date = 08/21/15 
 Pct Recovery = 98%  Analysis Date = 08/17/15 
 Pct Recovery = 98%  Analysis Date = 08/17/15 
 Pct Recovery = 98%  Analysis Date = 08/13/15 
 Pct Recovery = 98%  Analysis Date = 08/13/15 
 Pct Recovery = 98%  Analysis Date = 08/09/15 
 Pct Recovery = 99%  Analysis Date = 08/09/15 
 Pct Recovery = 99%  Analysis Date = 08/05/15 
 Pct Recovery = 99%  Analysis Date = 08/05/15 
 Pct Recovery = 99%  Analysis Date = 08/01/15 
 Pct Recovery = 100%  Analysis Date = 08/01/15 
 Pct Recovery = 100%  Analysis Date = 07/28/15 
 Pct Recovery = 100%  Analysis Date = 07/28/15 
 Pct Recovery = 100%  Analysis Date = 07/23/15 
 Pct Recovery = 101%  Analysis Date = 07/23/15 
 Pct Recovery = 101%  Analysis Date = 07/19/15 
 Pct Recovery = 101%  Analysis Date = 07/19/15 
 Pct Recovery = 101%  Analysis Date = 07/15/15 
 Pct Recovery = 102%  Analysis Date = 07/15/15 
 Pct Recovery = 102%  Analysis Date = 07/11/15 
 Pct Recovery = 102%  Analysis Date = 07/11/15 
 Pct Recovery = 102%  Analysis Date = 07/07/15 
 Pct Recovery = 102%  Analysis Date = 07/07/15 
 Pct Recovery = 102%  Analysis Date = 07/03/15 
 Pct Recovery = 103%  Analysis Date = 07/03/15 
 Pct Recovery = 103%  Analysis Date = 06/29/15 
 Pct Recovery = 103%  Analysis Date = 06/29/15 
 Pct Recovery = 103%  Analysis Date = 06/24/15 
 Pct Recovery = 104%  Analysis Date = 06/24/15 
 Pct Recovery = 104%  Analysis Date = 06/20/15 
 Pct Recovery = 104%  Analysis Date = 06/20/15 
 Pct Recovery = 104%  Analysis Date = 06/16/15 
 Pct Recovery = 105%  Analysis Date = 06/16/15 
 Pct Recovery = 105%  Analysis Date = 06/12/15 
 Pct Recovery = 105%  Analysis Date = 06/12/15 
 Pct Recovery = 105%  Analysis Date = 06/08/15 
 Pct Recovery = 105%  Analysis Date = 06/08/15 
 Pct Recovery = 105%  Analysis Date = 06/04/15 
 Pct Recovery = 105%  Analysis Date = 06/04/15 
 Pct Recovery = 105%  Analysis Date = 05/31/15 
 Pct Recovery = 106%  Analysis Date = 05/31/15 
 Pct Recovery = 106%  Analysis Date = 05/27/15 
 Pct Recovery = 106%  Analysis Date = 05/27/15 
 Pct Recovery = 106%  Analysis Date = 05/22/15 
 Pct Recovery = 106%  Analysis Date = 05/22/15 
 Pct Recovery = 106%  Analysis Date = 05/18/15 
 Pct Recovery = 106%  Analysis Date = 05/18/15 
 Pct Recovery = 106%  Analysis Date = 05/14/15 
 Pct Recovery = 107%  Analysis Date = 05/14/15 
 Pct Recovery = 107%  Analysis Date = 05/10/15 
 Pct Recovery = 107%  Analysis Date = 05/10/15 
 Pct Recovery = 107%  Analysis Date = 05/06/15 
 Pct Recovery = 107%  Analysis Date = 05/06/15 
 Pct Recovery = 107%  Analysis Date = 05/02/15 
 Pct Recovery = 107%  Analysis Date = 05/02/15 
 Pct Recovery = 107%  Analysis Date = 04/28/15 
 Pct Recovery = 107%  Analysis Date = 04/28/15 
 Pct Recovery = 107%  Analysis Date = 04/23/15 
 Pct Recovery = 108%  Analysis Date = 04/23/15 
 Pct Recovery = 108%  Analysis Date = 04/19/15 
 Pct Recovery = 108%  Analysis Date = 04/19/15 
 Pct Recovery = 108%  Analysis Date = 04/15/15 
 Pct Recovery = 108%  Analysis Date = 04/15/15 
 Pct Recovery = 108%  Analysis Date = 04/11/15 
 Pct Recovery = 108%  Analysis Date = 04/11/15 
 Pct Recovery = 108%  Analysis Date = 04/07/15 
 Pct Recovery = 108%  Analysis Date = 04/07/15 
 Pct Recovery = 108%  Analysis Date = 04/03/15 
 Pct Recovery = 109%  Analysis Date = 04/03/15 
 Pct Recovery = 109%  Analysis Date = 03/30/15 
 Pct Recovery = 109%  Analysis Date = 03/30/15 
 Pct Recovery = 109%  Analysis Date = 03/25/15 
 Pct Recovery = 109%  Analysis Date = 03/25/15 
 Pct Recovery = 109%  Analysis Date = 03/21/15 
 Pct Recovery = 109%  Analysis Date = 03/21/15 
 Pct Recovery = 109%  Analysis Date = 03/17/15 
 Pct Recovery = 109%  Analysis Date = 03/17/15 
 Pct Recovery = 109%  Analysis Date = 03/13/15 
 Pct Recovery = 109%  Analysis Date = 03/13/15 
 Pct Recovery = 109%  Analysis Date = 03/09/15 
 Pct Recovery = 109%  Analysis Date = 03/09/15 
 Pct Recovery = 109%  Analysis Date = 03/05/15 
 Pct Recovery = 109%  Analysis Date = 03/05/15 
 Pct Recovery = 109%  Analysis Date = 03/01/15 
 Pct Recovery = 109%  Analysis Date = 03/01/15 
 Pct Recovery = 109%  Analysis Date = 02/24/15 
 Pct Recovery = 110%  Analysis Date = 02/24/15 
 Pct Recovery = 110%  Analysis Date = 02/20/15 
 Pct Recovery = 110%  Analysis Date = 02/20/15 
 Pct Recovery = 110%  Analysis Date = 02/16/15 
 Pct Recovery = 110%  Analysis Date = 02/16/15 
 Pct Recovery = 110%  Analysis Date = 02/12/15 
 Pct Recovery = 110%  Analysis Date = 02/12/15 
 Pct Recovery = 110%  Analysis Date = 02/08/15 
 Pct Recovery = 110%  Analysis Date = 02/08/15 
 Pct Recovery = 110%  Analysis Date = 02/04/15 
 Pct Recovery = 110%  Analysis Date = 02/04/15 
 Pct Recovery = 110%  Analysis Date = 01/31/15 
 Pct Recovery = 110%  Analysis Date = 01/31/15 
 Pct Recovery = 110%  Analysis Date = 01/26/15 
 Pct Recovery = 110%  Analysis Date = 01/26/15 
 Pct Recovery = 110%  Analysis Date = 01/22/15 
 Pct Recovery = 110%  Analysis Date = 01/22/15 
 Pct Recovery = 110%  Analysis Date = 01/18/15 
 Pct Recovery = 110%  Analysis Date = 01/18/15 
 Pct Recovery = 110%  Analysis Date = 01/14/15 
 Pct Recovery = 110%  Analysis Date = 01/14/15 
 Pct Recovery = 110%  Analysis Date = 01/10/15 
 Pct Recovery = 110%  Analysis Date = 01/10/15 
 Pct Recovery = 110%  Analysis Date = 01/06/15 
 Pct Recovery = 110%  Analysis Date = 01/06/15 
 Pct Recovery = 110%  Analysis Date = 01/02/15 
 Pct Recovery = 110%  Analysis Date = 01/02/15 
 Pct Recovery = 110%  Analysis Date = 12/28/14 
 Pct Recovery = 110%  Analysis Date = 12/28/14 
 Pct Recovery = 110%  Analysis Date = 12/24/14 
 Pct Recovery = 110%  Analysis Date = 12/24/14 
 Pct Recovery = 110%  Analysis Date = 12/20/14 
 Pct Recovery = 110%  Analysis Date = 12/20/14 
 Pct Recovery = 110%  Analysis Date = 12/16/14 
 Pct Recovery = 110%  Analysis Date = 12/16/14 
 Pct Recovery = 110%  Analysis Date = 12/12/14 
 Pct Recovery = 110%  Analysis Date = 12/12/14 
 Pct Recovery = 110%  Analysis Date = 12/08/14 
 Pct Recovery = 110%  Analysis Date = 12/08/14 
 Pct Recovery = 110%  Analysis Date = 12/04/14 
 Pct Recovery = 109%  Analysis Date = 12/04/14 
 Pct Recovery = 109%  Analysis Date = 11/29/14 
 Pct Recovery = 109%  Analysis Date = 11/29/14 
 Pct Recovery = 109%  Analysis Date = 11/25/14 
 Pct Recovery = 109%  Analysis Date = 11/25/14 
 Pct Recovery = 109%  Analysis Date = 11/21/14 
 Pct Recovery = 109%  Analysis Date = 11/21/14 
 Pct Recovery = 109%  Analysis Date = 11/17/14 
 Pct Recovery = 109%  Analysis Date = 11/17/14 
 Pct Recovery = 109%  Analysis Date = 11/13/14 
 Pct Recovery = 108%  Analysis Date = 11/13/14 
 Pct Recovery = 108%  Analysis Date = 11/09/14 
 Pct Recovery = 108%  Analysis Date = 11/09/14 
 Pct Recovery = 108%  Analysis Date = 11/05/14 
 Pct Recovery = 108%  Analysis Date = 11/05/14 
 Pct Recovery = 108%  Analysis Date = 11/01/14 
 Pct Recovery = 108%  Analysis Date = 11/01/14 
 Pct Recovery = 108%  Analysis Date = 10/27/14 
 Pct Recovery = 108%  Analysis Date = 10/27/14 
 Pct Recovery = 108%  Analysis Date = 10/23/14 
 Pct Recovery = 108%  Analysis Date = 10/23/14 
 Pct Recovery = 108%  Analysis Date = 10/19/14 
 Pct Recovery = 107%  Analysis Date = 10/19/14 
 Pct Recovery = 107%  Analysis Date = 10/15/14 
 Pct Recovery = 107%  Analysis Date = 10/15/14 
 Pct Recovery = 107%  Analysis Date = 10/11/14 
 Pct Recovery = 107%  Analysis Date = 10/11/14 
 Pct Recovery = 107%  Analysis Date = 10/07/14 
 Pct Recovery = 107%  Analysis Date = 10/07/14 
 Pct Recovery = 107%  Analysis Date = 10/03/14 
 Pct Recovery = 107%  Analysis Date = 10/03/14 
 Pct Recovery = 107%  Analysis Date = 09/28/14 
 Pct Recovery = 107%  Analysis Date = 09/28/14 
 Pct Recovery = 107%  Analysis Date = 09/24/14 
 Pct Recovery = 106%  Analysis Date = 09/24/14 
 Pct Recovery = 106%  Analysis Date = 09/20/14 
 Pct Recovery = 106%  Analysis Date = 09/20/14 
 Pct Recovery = 106%  Analysis Date = 09/16/14 
 Pct Recovery = 106%  Analysis Date = 09/16/14 
 Pct Recovery = 106%  Analysis Date = 09/12/14 
 Pct Recovery = 106%  Analysis Date = 09/12/14 
 Pct Recovery = 106%  Analysis Date = 09/08/14 
 Pct Recovery = 106%  Analysis Date = 09/08/14 
 Pct Recovery = 106%  Analysis Date = 09/04/14 
 Pct Recovery = 106%  Analysis Date = 09/04/14 
 Pct Recovery = 106%  Analysis Date = 08/30/14 
 Pct Recovery = 105%  Analysis Date = 08/30/14 
 Pct Recovery = 105%  Analysis Date = 08/26/14 
 Pct Recovery = 105%  Analysis Date = 08/26/14 
 Pct Recovery = 105%  Analysis Date = 08/22/14 
 Pct Recovery = 105%  Analysis Date = 08/22/14 
 Pct Recovery = 105%  Analysis Date = 08/18/14 
 Pct Recovery = 105%  Analysis Date = 08/18/14 
 Pct Recovery = 105%  Analysis Date = 08/14/14 
 Pct Recovery = 105%  Analysis Date = 08/14/14 
 Pct Recovery = 105%  Analysis Date = 08/10/14 
 Pct Recovery = 105%  Analysis Date = 08/10/14 
 Pct Recovery = 105%  Analysis Date = 08/06/14 
 Pct Recovery = 104%  Analysis Date = 08/06/14 
 Pct Recovery = 104%  Analysis Date = 08/01/14 
 Pct Recovery = 104%  Analysis Date = 08/01/14 
 Pct Recovery = 104%  Analysis Date = 07/28/14 
 Pct Recovery = 104%  Analysis Date = 07/28/14 
 Pct Recovery = 104%  Analysis Date = 07/24/14 
 Pct Recovery = 104%  Analysis Date = 07/24/14 
 Pct Recovery = 104%  Analysis Date = 07/20/14 
 Pct Recovery = 104%  Analysis Date = 07/20/14 
 Pct Recovery = 104%  Analysis Date = 07/16/14 
 Pct Recovery = 104%  Analysis Date = 07/16/14 
 Pct Recovery = 104%  Analysis Date = 07/12/14 
 Pct Recovery = 103%  Analysis Date = 07/12/14 
 Pct Recovery = 103%  Analysis Date = 07/08/14 
 Pct Recovery = 103%  Analysis Date = 07/08/14 
 Pct Recovery = 103%  Analysis Date = 07/03/14 
 Pct Recovery = 103%  Analysis Date = 07/03/14 
 Pct Recovery = 103%  Analysis Date = 06/29/14 
 Pct Recovery = 103%  Analysis Date = 06/29/14 
 Pct Recovery = 103%  Analysis Date = 06/25/14 
 Pct Recovery = 103%  Analysis Date = 06/25/14 
 Pct Recovery = 103%  Analysis Date = 06/21/14 
 Pct Recovery = 103%  Analysis Date = 06/21/14 
 Pct Recovery = 103%  Analysis Date = 06/17/14 
 Pct Recovery = 103%  Analysis Date = 06/17/14 
 Pct Recovery = 103%  Analysis Date = 06/13/14 
 Pct Recovery = 102%  Analysis Date = 06/13/14 
 Pct Recovery = 102%  Analysis Date = 06/09/14 
 Pct Recovery = 102%  Analysis Date = 06/09/14 
 Pct Recovery = 102%  Analysis Date = 06/04/14 
 Pct Recovery = 102%  Analysis Date = 06/04/14 
 Pct Recovery = 102%  Analysis Date = 05/31/14 
 Pct Recovery = 102%  Analysis Date = 05/31/14 
 Pct Recovery = 102%  Analysis Date = 05/27/14 
 Pct Recovery = 102%  Analysis Date = 05/27/14 
 Pct Recovery = 102%  Analysis Date = 05/23/14 
 Pct Recovery = 102%  Analysis Date = 05/23/14 
 Pct Recovery = 102%  Analysis Date = 05/19/14 
 Pct Recovery = 101%  Analysis Date = 05/19/14 
 Pct Recovery = 101%  Analysis Date = 05/15/14 
 Pct Recovery = 101%  Analysis Date = 05/15/14 
 Pct Recovery = 101%  Analysis Date = 05/11/14 
 Pct Recovery = 101%  Analysis Date = 05/11/14 
 Pct Recovery = 101%  Analysis Date = 05/07/14 
 Pct Recovery = 101%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
TERT-BUTYL ALCOHOL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 28 101% 11% 100% 7%
Total 28 101% 11% 100% 7%

Sample Statistics
TERT-BUTYL ALCOHOL

Characteristic N % % Basis
Plotted 28 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 28 .  
False Negatives 0 0% 0 out of 28
Not Spiked 20 .  
False Positives 0 0% 0 out of 20

BQS OBSP Determination:
TERT-BUTYL METHYL ETHER (MTBE)
METHOD: 4437 , TESTIDCODE: 78032GM016
Open Data Set

 Analysis Date = 07/29/16 
 SpikeMix = Supelco LC20145V: 40 µl & NSI 041516: 40 µl & NSI 041416HVOC: 40 µl 
 Pct Recovery = 139%  Analysis Date = 07/06/16 
 SpikeMix = Accu 216041354: 40 µl & NSI 041516: 40 µl & NSI 041416HVOC: 40 µl 
 Pct Recovery = 111%  Analysis Date = 08/11/16 
 SpikeMix = Phenova B20160303: 25 µl & Supelco LC20145V: 25 µl & NSI 041416HVOC: 25 µl 
 Pct Recovery = 161%  Analysis Date = 05/21/16 
 SpikeMix = Supelco LC20145V: 25 µl & NSI 041516: 25 µl & NSI 041416HVOC: 25 µl 
 Pct Recovery = 140%  Analysis Date = 07/11/14 
 SpikeMix = ChemService 2615700: 20 µl & Accu 214031128: 20 µl 
 Pct Recovery = 134%  Analysis Date = 07/03/14 
 SpikeMix = Abs 032014: 20 µl & ChemService 2615700: 20 µl 
 Pct Recovery = 110%  Analysis Date = 06/07/14 
 SpikeMix = ChemService 2615700: 20 µl & Supelco LC06437: 20 µl 
 Pct Recovery = 98%  Analysis Date = 06/06/14 
 SpikeMix = NSI 031814: 20 µl & ChemService 2615700: 20 µl 
 Pct Recovery = 97%  Analysis Date = 08/13/14 
 SpikeMix = ERA 0321-14-05: 20 µl & Accu 214031128: 20 µl 
 Pct Recovery = 162%  Analysis Date = 10/09/15 
 SpikeMix = Supelco LC13544: 25 µl & NSI 050515HVOC: 25 µl 
 Pct Recovery = 110%  Analysis Date = 10/09/15 
 SpikeMix = ERA 0601-15-05: 25 µl & Accu 215041338: 25 µl 
 Pct Recovery = 94%  Analysis Date = 06/26/15 
 SpikeMix = ChemService 3818700: 25 µl & Accu 215041338: 25 µl 
 Pct Recovery = 97%  Analysis Date = 08/12/16 
 SpikeMix = Accu 216041354: 15 µl & Abs 060916HVOC: 15 µl 
 Pct Recovery = 95%  Analysis Date = 07/06/16 
 SpikeMix = Phenova B20160303: 15 µl & Accu 216041354: 15 µl & NSI 041416HVOC: 15 µl 
 Pct Recovery = 134%  Analysis Date = 06/23/16 
 SpikeMix = . 
 Pct Recovery = 119%  Analysis Date = 05/20/16 
 SpikeMix = Accu 216041354: 15 µl & NSI 041516: 15 µl & Accu 216041225: 15 µl 
 Pct Recovery = 123%  Analysis Date = 04/28/16 
 SpikeMix = ChemService 3818700: 15 µl & Supelco LC13544: 15 µl 
 Pct Recovery = 111%  Analysis Date = 07/30/15 
 SpikeMix = Supelco LC13544: 15 µl & NSI 050515HVOC: 15 µl 
 Pct Recovery = 116%  Analysis Date = 05/14/15 
 SpikeMix = ChemService 3818700: 15 µl & Supelco LC13544: 15 µl 
 Pct Recovery = 121%  Analysis Date = 11/25/15 
 SpikeMix = Accu 215041338: 15 µl & Abs 040315: 15 µl 
 Pct Recovery = 96%  Analysis Date = 09/05/15 
 SpikeMix = Accu 215041338: 15 µl & NSI 050515HVOC: 15 µl 
 Pct Recovery = 95%  Analysis Date = 11/22/14 
 SpikeMix = ChemService 2615700: 10 µl & Supelco LC06437: 10 µl 
 Pct Recovery = 90%  Analysis Date = 07/30/14 
 SpikeMix = NSI 031814: 10 µl & ChemService 2615700: 10 µl 
 Pct Recovery = 86%  Analysis Date = 05/20/14 
 SpikeMix = ChemService 2615700: 10 µl & Accu 214031128: 10 µl 
 Pct Recovery = 150%  Analysis Date = 04/25/15 
 SpikeMix = Abs 032014: 10 µl & ERA 0321-14-05A: 10 µl 
 Pct Recovery = 114%  Analysis Date = 10/21/14 
 SpikeMix = ERA 0321-14-05A: 10 µl & Accu 214031128: 10 µl 
 Pct Recovery = 167%  Analysis Date = 09/06/14 
 SpikeMix = ERA 0321-14-05: 10 µl & Supelco LC06437: 10 µl 
 Pct Recovery = 105%  Analysis Date = 03/22/16 
 SpikeMix = Supelco LC13544: 10 µl & NSI 050515HVOC: 10 µl 
 Pct Recovery = 123%  Analysis Date = 12/10/15 
 SpikeMix = ChemService 3818700: 10 µl & Supelco LC13544: 10 µl 
 Pct Recovery = 106%  Analysis Date = 05/05/15 
 SpikeMix = Supelco LC13544: 10 µl & Abs 040315: 10 µl 
 Pct Recovery = 117%  Analysis Date = 02/12/16 
 SpikeMix = ERA 0601-15-05: 10 µl & Accu 215041338: 10 µl 
 Pct Recovery = 95%  Analysis Date = 01/05/16 
 SpikeMix = Accu 215041338: 10 µl & Abs 040315: 10 µl 
 Pct Recovery = 103%  Analysis Date = 08/12/16 
 Pct Recovery = 131%  Analysis Date = 08/07/16 
 Pct Recovery = 131%  Analysis Date = 08/07/16 
 Pct Recovery = 131%  Analysis Date = 08/03/16 
 Pct Recovery = 130%  Analysis Date = 08/03/16 
 Pct Recovery = 130%  Analysis Date = 07/30/16 
 Pct Recovery = 130%  Analysis Date = 07/30/16 
 Pct Recovery = 130%  Analysis Date = 07/26/16 
 Pct Recovery = 129%  Analysis Date = 07/26/16 
 Pct Recovery = 129%  Analysis Date = 07/22/16 
 Pct Recovery = 129%  Analysis Date = 07/22/16 
 Pct Recovery = 129%  Analysis Date = 07/18/16 
 Pct Recovery = 128%  Analysis Date = 07/18/16 
 Pct Recovery = 128%  Analysis Date = 07/14/16 
 Pct Recovery = 128%  Analysis Date = 07/14/16 
 Pct Recovery = 128%  Analysis Date = 07/10/16 
 Pct Recovery = 127%  Analysis Date = 07/10/16 
 Pct Recovery = 127%  Analysis Date = 07/06/16 
 Pct Recovery = 127%  Analysis Date = 07/06/16 
 Pct Recovery = 127%  Analysis Date = 07/02/16 
 Pct Recovery = 126%  Analysis Date = 07/02/16 
 Pct Recovery = 126%  Analysis Date = 06/28/16 
 Pct Recovery = 126%  Analysis Date = 06/28/16 
 Pct Recovery = 126%  Analysis Date = 06/24/16 
 Pct Recovery = 125%  Analysis Date = 06/24/16 
 Pct Recovery = 125%  Analysis Date = 06/20/16 
 Pct Recovery = 125%  Analysis Date = 06/20/16 
 Pct Recovery = 125%  Analysis Date = 06/15/16 
 Pct Recovery = 124%  Analysis Date = 06/15/16 
 Pct Recovery = 124%  Analysis Date = 06/11/16 
 Pct Recovery = 124%  Analysis Date = 06/11/16 
 Pct Recovery = 124%  Analysis Date = 06/07/16 
 Pct Recovery = 123%  Analysis Date = 06/07/16 
 Pct Recovery = 123%  Analysis Date = 06/03/16 
 Pct Recovery = 123%  Analysis Date = 06/03/16 
 Pct Recovery = 123%  Analysis Date = 05/30/16 
 Pct Recovery = 123%  Analysis Date = 05/30/16 
 Pct Recovery = 123%  Analysis Date = 05/26/16 
 Pct Recovery = 122%  Analysis Date = 05/26/16 
 Pct Recovery = 122%  Analysis Date = 05/22/16 
 Pct Recovery = 122%  Analysis Date = 05/22/16 
 Pct Recovery = 122%  Analysis Date = 05/18/16 
 Pct Recovery = 121%  Analysis Date = 05/18/16 
 Pct Recovery = 121%  Analysis Date = 05/14/16 
 Pct Recovery = 121%  Analysis Date = 05/14/16 
 Pct Recovery = 121%  Analysis Date = 05/10/16 
 Pct Recovery = 120%  Analysis Date = 05/10/16 
 Pct Recovery = 120%  Analysis Date = 05/06/16 
 Pct Recovery = 120%  Analysis Date = 05/06/16 
 Pct Recovery = 120%  Analysis Date = 05/02/16 
 Pct Recovery = 119%  Analysis Date = 05/02/16 
 Pct Recovery = 119%  Analysis Date = 04/28/16 
 Pct Recovery = 119%  Analysis Date = 04/28/16 
 Pct Recovery = 119%  Analysis Date = 04/23/16 
 Pct Recovery = 118%  Analysis Date = 04/23/16 
 Pct Recovery = 118%  Analysis Date = 04/19/16 
 Pct Recovery = 118%  Analysis Date = 04/19/16 
 Pct Recovery = 118%  Analysis Date = 04/15/16 
 Pct Recovery = 117%  Analysis Date = 04/15/16 
 Pct Recovery = 117%  Analysis Date = 04/11/16 
 Pct Recovery = 117%  Analysis Date = 04/11/16 
 Pct Recovery = 117%  Analysis Date = 04/07/16 
 Pct Recovery = 117%  Analysis Date = 04/07/16 
 Pct Recovery = 117%  Analysis Date = 04/03/16 
 Pct Recovery = 116%  Analysis Date = 04/03/16 
 Pct Recovery = 116%  Analysis Date = 03/30/16 
 Pct Recovery = 116%  Analysis Date = 03/30/16 
 Pct Recovery = 116%  Analysis Date = 03/26/16 
 Pct Recovery = 115%  Analysis Date = 03/26/16 
 Pct Recovery = 115%  Analysis Date = 03/22/16 
 Pct Recovery = 115%  Analysis Date = 03/22/16 
 Pct Recovery = 115%  Analysis Date = 03/18/16 
 Pct Recovery = 114%  Analysis Date = 03/18/16 
 Pct Recovery = 114%  Analysis Date = 03/14/16 
 Pct Recovery = 114%  Analysis Date = 03/14/16 
 Pct Recovery = 114%  Analysis Date = 03/10/16 
 Pct Recovery = 113%  Analysis Date = 03/10/16 
 Pct Recovery = 113%  Analysis Date = 03/06/16 
 Pct Recovery = 113%  Analysis Date = 03/06/16 
 Pct Recovery = 113%  Analysis Date = 03/02/16 
 Pct Recovery = 113%  Analysis Date = 03/02/16 
 Pct Recovery = 113%  Analysis Date = 02/26/16 
 Pct Recovery = 112%  Analysis Date = 02/26/16 
 Pct Recovery = 112%  Analysis Date = 02/22/16 
 Pct Recovery = 112%  Analysis Date = 02/22/16 
 Pct Recovery = 112%  Analysis Date = 02/18/16 
 Pct Recovery = 111%  Analysis Date = 02/18/16 
 Pct Recovery = 111%  Analysis Date = 02/14/16 
 Pct Recovery = 111%  Analysis Date = 02/14/16 
 Pct Recovery = 111%  Analysis Date = 02/10/16 
 Pct Recovery = 110%  Analysis Date = 02/10/16 
 Pct Recovery = 110%  Analysis Date = 02/06/16 
 Pct Recovery = 110%  Analysis Date = 02/06/16 
 Pct Recovery = 110%  Analysis Date = 02/02/16 
 Pct Recovery = 110%  Analysis Date = 02/02/16 
 Pct Recovery = 110%  Analysis Date = 01/29/16 
 Pct Recovery = 109%  Analysis Date = 01/29/16 
 Pct Recovery = 109%  Analysis Date = 01/25/16 
 Pct Recovery = 109%  Analysis Date = 01/25/16 
 Pct Recovery = 109%  Analysis Date = 01/21/16 
 Pct Recovery = 109%  Analysis Date = 01/21/16 
 Pct Recovery = 109%  Analysis Date = 01/17/16 
 Pct Recovery = 108%  Analysis Date = 01/17/16 
 Pct Recovery = 108%  Analysis Date = 01/13/16 
 Pct Recovery = 108%  Analysis Date = 01/13/16 
 Pct Recovery = 108%  Analysis Date = 01/09/16 
 Pct Recovery = 108%  Analysis Date = 01/09/16 
 Pct Recovery = 108%  Analysis Date = 01/04/16 
 Pct Recovery = 107%  Analysis Date = 01/04/16 
 Pct Recovery = 107%  Analysis Date = 12/31/15 
 Pct Recovery = 107%  Analysis Date = 12/31/15 
 Pct Recovery = 107%  Analysis Date = 12/27/15 
 Pct Recovery = 107%  Analysis Date = 12/27/15 
 Pct Recovery = 107%  Analysis Date = 12/23/15 
 Pct Recovery = 106%  Analysis Date = 12/23/15 
 Pct Recovery = 106%  Analysis Date = 12/19/15 
 Pct Recovery = 106%  Analysis Date = 12/19/15 
 Pct Recovery = 106%  Analysis Date = 12/15/15 
 Pct Recovery = 106%  Analysis Date = 12/15/15 
 Pct Recovery = 106%  Analysis Date = 12/11/15 
 Pct Recovery = 105%  Analysis Date = 12/11/15 
 Pct Recovery = 105%  Analysis Date = 12/07/15 
 Pct Recovery = 105%  Analysis Date = 12/07/15 
 Pct Recovery = 105%  Analysis Date = 12/03/15 
 Pct Recovery = 105%  Analysis Date = 12/03/15 
 Pct Recovery = 105%  Analysis Date = 11/29/15 
 Pct Recovery = 105%  Analysis Date = 11/29/15 
 Pct Recovery = 105%  Analysis Date = 11/25/15 
 Pct Recovery = 105%  Analysis Date = 11/25/15 
 Pct Recovery = 105%  Analysis Date = 11/21/15 
 Pct Recovery = 105%  Analysis Date = 11/21/15 
 Pct Recovery = 105%  Analysis Date = 11/17/15 
 Pct Recovery = 105%  Analysis Date = 11/17/15 
 Pct Recovery = 105%  Analysis Date = 11/12/15 
 Pct Recovery = 105%  Analysis Date = 11/12/15 
 Pct Recovery = 105%  Analysis Date = 11/08/15 
 Pct Recovery = 105%  Analysis Date = 11/08/15 
 Pct Recovery = 105%  Analysis Date = 11/04/15 
 Pct Recovery = 105%  Analysis Date = 11/04/15 
 Pct Recovery = 105%  Analysis Date = 10/31/15 
 Pct Recovery = 105%  Analysis Date = 10/31/15 
 Pct Recovery = 105%  Analysis Date = 10/27/15 
 Pct Recovery = 105%  Analysis Date = 10/27/15 
 Pct Recovery = 105%  Analysis Date = 10/23/15 
 Pct Recovery = 105%  Analysis Date = 10/23/15 
 Pct Recovery = 105%  Analysis Date = 10/19/15 
 Pct Recovery = 105%  Analysis Date = 10/19/15 
 Pct Recovery = 105%  Analysis Date = 10/15/15 
 Pct Recovery = 105%  Analysis Date = 10/15/15 
 Pct Recovery = 105%  Analysis Date = 10/11/15 
 Pct Recovery = 105%  Analysis Date = 10/11/15 
 Pct Recovery = 105%  Analysis Date = 10/07/15 
 Pct Recovery = 106%  Analysis Date = 10/07/15 
 Pct Recovery = 106%  Analysis Date = 10/03/15 
 Pct Recovery = 106%  Analysis Date = 10/03/15 
 Pct Recovery = 106%  Analysis Date = 09/29/15 
 Pct Recovery = 106%  Analysis Date = 09/29/15 
 Pct Recovery = 106%  Analysis Date = 09/25/15 
 Pct Recovery = 106%  Analysis Date = 09/25/15 
 Pct Recovery = 106%  Analysis Date = 09/21/15 
 Pct Recovery = 106%  Analysis Date = 09/21/15 
 Pct Recovery = 106%  Analysis Date = 09/16/15 
 Pct Recovery = 106%  Analysis Date = 09/16/15 
 Pct Recovery = 106%  Analysis Date = 09/12/15 
 Pct Recovery = 106%  Analysis Date = 09/12/15 
 Pct Recovery = 106%  Analysis Date = 09/08/15 
 Pct Recovery = 106%  Analysis Date = 09/08/15 
 Pct Recovery = 106%  Analysis Date = 09/04/15 
 Pct Recovery = 107%  Analysis Date = 09/04/15 
 Pct Recovery = 107%  Analysis Date = 08/31/15 
 Pct Recovery = 107%  Analysis Date = 08/31/15 
 Pct Recovery = 107%  Analysis Date = 08/27/15 
 Pct Recovery = 107%  Analysis Date = 08/27/15 
 Pct Recovery = 107%  Analysis Date = 08/23/15 
 Pct Recovery = 107%  Analysis Date = 08/23/15 
 Pct Recovery = 107%  Analysis Date = 08/19/15 
 Pct Recovery = 107%  Analysis Date = 08/19/15 
 Pct Recovery = 107%  Analysis Date = 08/15/15 
 Pct Recovery = 107%  Analysis Date = 08/15/15 
 Pct Recovery = 107%  Analysis Date = 08/11/15 
 Pct Recovery = 107%  Analysis Date = 08/11/15 
 Pct Recovery = 107%  Analysis Date = 08/07/15 
 Pct Recovery = 108%  Analysis Date = 08/07/15 
 Pct Recovery = 108%  Analysis Date = 08/03/15 
 Pct Recovery = 108%  Analysis Date = 08/03/15 
 Pct Recovery = 108%  Analysis Date = 07/30/15 
 Pct Recovery = 108%  Analysis Date = 07/30/15 
 Pct Recovery = 108%  Analysis Date = 07/25/15 
 Pct Recovery = 108%  Analysis Date = 07/25/15 
 Pct Recovery = 108%  Analysis Date = 07/21/15 
 Pct Recovery = 108%  Analysis Date = 07/21/15 
 Pct Recovery = 108%  Analysis Date = 07/17/15 
 Pct Recovery = 108%  Analysis Date = 07/17/15 
 Pct Recovery = 108%  Analysis Date = 07/13/15 
 Pct Recovery = 109%  Analysis Date = 07/13/15 
 Pct Recovery = 109%  Analysis Date = 07/09/15 
 Pct Recovery = 109%  Analysis Date = 07/09/15 
 Pct Recovery = 109%  Analysis Date = 07/05/15 
 Pct Recovery = 109%  Analysis Date = 07/05/15 
 Pct Recovery = 109%  Analysis Date = 07/01/15 
 Pct Recovery = 109%  Analysis Date = 07/01/15 
 Pct Recovery = 109%  Analysis Date = 06/27/15 
 Pct Recovery = 109%  Analysis Date = 06/27/15 
 Pct Recovery = 109%  Analysis Date = 06/23/15 
 Pct Recovery = 109%  Analysis Date = 06/23/15 
 Pct Recovery = 109%  Analysis Date = 06/19/15 
 Pct Recovery = 110%  Analysis Date = 06/19/15 
 Pct Recovery = 110%  Analysis Date = 06/15/15 
 Pct Recovery = 110%  Analysis Date = 06/15/15 
 Pct Recovery = 110%  Analysis Date = 06/11/15 
 Pct Recovery = 110%  Analysis Date = 06/11/15 
 Pct Recovery = 110%  Analysis Date = 06/07/15 
 Pct Recovery = 110%  Analysis Date = 06/07/15 
 Pct Recovery = 110%  Analysis Date = 06/02/15 
 Pct Recovery = 111%  Analysis Date = 06/02/15 
 Pct Recovery = 111%  Analysis Date = 05/29/15 
 Pct Recovery = 111%  Analysis Date = 05/29/15 
 Pct Recovery = 111%  Analysis Date = 05/25/15 
 Pct Recovery = 111%  Analysis Date = 05/25/15 
 Pct Recovery = 111%  Analysis Date = 05/21/15 
 Pct Recovery = 111%  Analysis Date = 05/21/15 
 Pct Recovery = 111%  Analysis Date = 05/17/15 
 Pct Recovery = 111%  Analysis Date = 05/17/15 
 Pct Recovery = 111%  Analysis Date = 05/13/15 
 Pct Recovery = 112%  Analysis Date = 05/13/15 
 Pct Recovery = 112%  Analysis Date = 05/09/15 
 Pct Recovery = 112%  Analysis Date = 05/09/15 
 Pct Recovery = 112%  Analysis Date = 05/05/15 
 Pct Recovery = 112%  Analysis Date = 05/05/15 
 Pct Recovery = 112%  Analysis Date = 05/01/15 
 Pct Recovery = 112%  Analysis Date = 05/01/15 
 Pct Recovery = 112%  Analysis Date = 04/27/15 
 Pct Recovery = 113%  Analysis Date = 04/27/15 
 Pct Recovery = 113%  Analysis Date = 04/23/15 
 Pct Recovery = 113%  Analysis Date = 04/23/15 
 Pct Recovery = 113%  Analysis Date = 04/19/15 
 Pct Recovery = 113%  Analysis Date = 04/19/15 
 Pct Recovery = 113%  Analysis Date = 04/15/15 
 Pct Recovery = 113%  Analysis Date = 04/15/15 
 Pct Recovery = 113%  Analysis Date = 04/11/15 
 Pct Recovery = 113%  Analysis Date = 04/11/15 
 Pct Recovery = 113%  Analysis Date = 04/06/15 
 Pct Recovery = 113%  Analysis Date = 04/06/15 
 Pct Recovery = 113%  Analysis Date = 04/02/15 
 Pct Recovery = 113%  Analysis Date = 04/02/15 
 Pct Recovery = 113%  Analysis Date = 03/29/15 
 Pct Recovery = 113%  Analysis Date = 03/29/15 
 Pct Recovery = 113%  Analysis Date = 03/25/15 
 Pct Recovery = 114%  Analysis Date = 03/25/15 
 Pct Recovery = 114%  Analysis Date = 03/21/15 
 Pct Recovery = 114%  Analysis Date = 03/21/15 
 Pct Recovery = 114%  Analysis Date = 03/17/15 
 Pct Recovery = 114%  Analysis Date = 03/17/15 
 Pct Recovery = 114%  Analysis Date = 03/13/15 
 Pct Recovery = 114%  Analysis Date = 03/13/15 
 Pct Recovery = 114%  Analysis Date = 03/09/15 
 Pct Recovery = 114%  Analysis Date = 03/09/15 
 Pct Recovery = 114%  Analysis Date = 03/05/15 
 Pct Recovery = 114%  Analysis Date = 03/05/15 
 Pct Recovery = 114%  Analysis Date = 03/01/15 
 Pct Recovery = 114%  Analysis Date = 03/01/15 
 Pct Recovery = 114%  Analysis Date = 02/25/15 
 Pct Recovery = 114%  Analysis Date = 02/25/15 
 Pct Recovery = 114%  Analysis Date = 02/21/15 
 Pct Recovery = 115%  Analysis Date = 02/21/15 
 Pct Recovery = 115%  Analysis Date = 02/17/15 
 Pct Recovery = 115%  Analysis Date = 02/17/15 
 Pct Recovery = 115%  Analysis Date = 02/12/15 
 Pct Recovery = 115%  Analysis Date = 02/12/15 
 Pct Recovery = 115%  Analysis Date = 02/08/15 
 Pct Recovery = 115%  Analysis Date = 02/08/15 
 Pct Recovery = 115%  Analysis Date = 02/04/15 
 Pct Recovery = 115%  Analysis Date = 02/04/15 
 Pct Recovery = 115%  Analysis Date = 01/31/15 
 Pct Recovery = 115%  Analysis Date = 01/31/15 
 Pct Recovery = 115%  Analysis Date = 01/27/15 
 Pct Recovery = 115%  Analysis Date = 01/27/15 
 Pct Recovery = 115%  Analysis Date = 01/23/15 
 Pct Recovery = 116%  Analysis Date = 01/23/15 
 Pct Recovery = 116%  Analysis Date = 01/19/15 
 Pct Recovery = 116%  Analysis Date = 01/19/15 
 Pct Recovery = 116%  Analysis Date = 01/15/15 
 Pct Recovery = 116%  Analysis Date = 01/15/15 
 Pct Recovery = 116%  Analysis Date = 01/11/15 
 Pct Recovery = 116%  Analysis Date = 01/11/15 
 Pct Recovery = 116%  Analysis Date = 01/07/15 
 Pct Recovery = 116%  Analysis Date = 01/07/15 
 Pct Recovery = 116%  Analysis Date = 01/03/15 
 Pct Recovery = 116%  Analysis Date = 01/03/15 
 Pct Recovery = 116%  Analysis Date = 12/30/14 
 Pct Recovery = 116%  Analysis Date = 12/30/14 
 Pct Recovery = 116%  Analysis Date = 12/26/14 
 Pct Recovery = 116%  Analysis Date = 12/26/14 
 Pct Recovery = 116%  Analysis Date = 12/21/14 
 Pct Recovery = 117%  Analysis Date = 12/21/14 
 Pct Recovery = 117%  Analysis Date = 12/17/14 
 Pct Recovery = 117%  Analysis Date = 12/17/14 
 Pct Recovery = 117%  Analysis Date = 12/13/14 
 Pct Recovery = 117%  Analysis Date = 12/13/14 
 Pct Recovery = 117%  Analysis Date = 12/09/14 
 Pct Recovery = 117%  Analysis Date = 12/09/14 
 Pct Recovery = 117%  Analysis Date = 12/05/14 
 Pct Recovery = 117%  Analysis Date = 12/05/14 
 Pct Recovery = 117%  Analysis Date = 12/01/14 
 Pct Recovery = 117%  Analysis Date = 12/01/14 
 Pct Recovery = 117%  Analysis Date = 11/27/14 
 Pct Recovery = 117%  Analysis Date = 11/27/14 
 Pct Recovery = 117%  Analysis Date = 11/23/14 
 Pct Recovery = 118%  Analysis Date = 11/23/14 
 Pct Recovery = 118%  Analysis Date = 11/19/14 
 Pct Recovery = 118%  Analysis Date = 11/19/14 
 Pct Recovery = 118%  Analysis Date = 11/15/14 
 Pct Recovery = 118%  Analysis Date = 11/15/14 
 Pct Recovery = 118%  Analysis Date = 11/11/14 
 Pct Recovery = 118%  Analysis Date = 11/11/14 
 Pct Recovery = 118%  Analysis Date = 11/07/14 
 Pct Recovery = 118%  Analysis Date = 11/07/14 
 Pct Recovery = 118%  Analysis Date = 11/03/14 
 Pct Recovery = 118%  Analysis Date = 11/03/14 
 Pct Recovery = 118%  Analysis Date = 10/30/14 
 Pct Recovery = 118%  Analysis Date = 10/30/14 
 Pct Recovery = 118%  Analysis Date = 10/25/14 
 Pct Recovery = 118%  Analysis Date = 10/25/14 
 Pct Recovery = 118%  Analysis Date = 10/21/14 
 Pct Recovery = 118%  Analysis Date = 10/21/14 
 Pct Recovery = 118%  Analysis Date = 10/17/14 
 Pct Recovery = 118%  Analysis Date = 10/17/14 
 Pct Recovery = 118%  Analysis Date = 10/13/14 
 Pct Recovery = 118%  Analysis Date = 10/13/14 
 Pct Recovery = 118%  Analysis Date = 10/09/14 
 Pct Recovery = 118%  Analysis Date = 10/09/14 
 Pct Recovery = 118%  Analysis Date = 10/05/14 
 Pct Recovery = 118%  Analysis Date = 10/05/14 
 Pct Recovery = 118%  Analysis Date = 10/01/14 
 Pct Recovery = 119%  Analysis Date = 10/01/14 
 Pct Recovery = 119%  Analysis Date = 09/27/14 
 Pct Recovery = 119%  Analysis Date = 09/27/14 
 Pct Recovery = 119%  Analysis Date = 09/23/14 
 Pct Recovery = 119%  Analysis Date = 09/23/14 
 Pct Recovery = 119%  Analysis Date = 09/19/14 
 Pct Recovery = 119%  Analysis Date = 09/19/14 
 Pct Recovery = 119%  Analysis Date = 09/15/14 
 Pct Recovery = 119%  Analysis Date = 09/15/14 
 Pct Recovery = 119%  Analysis Date = 09/11/14 
 Pct Recovery = 119%  Analysis Date = 09/11/14 
 Pct Recovery = 119%  Analysis Date = 09/07/14 
 Pct Recovery = 119%  Analysis Date = 09/07/14 
 Pct Recovery = 119%  Analysis Date = 09/02/14 
 Pct Recovery = 119%  Analysis Date = 09/02/14 
 Pct Recovery = 119%  Analysis Date = 08/29/14 
 Pct Recovery = 119%  Analysis Date = 08/29/14 
 Pct Recovery = 119%  Analysis Date = 08/25/14 
 Pct Recovery = 119%  Analysis Date = 08/25/14 
 Pct Recovery = 119%  Analysis Date = 08/21/14 
 Pct Recovery = 119%  Analysis Date = 08/21/14 
 Pct Recovery = 119%  Analysis Date = 08/17/14 
 Pct Recovery = 119%  Analysis Date = 08/17/14 
 Pct Recovery = 119%  Analysis Date = 08/13/14 
 Pct Recovery = 119%  Analysis Date = 08/13/14 
 Pct Recovery = 119%  Analysis Date = 08/09/14 
 Pct Recovery = 119%  Analysis Date = 08/09/14 
 Pct Recovery = 119%  Analysis Date = 08/05/14 
 Pct Recovery = 120%  Analysis Date = 08/05/14 
 Pct Recovery = 120%  Analysis Date = 08/01/14 
 Pct Recovery = 120%  Analysis Date = 08/01/14 
 Pct Recovery = 120%  Analysis Date = 07/28/14 
 Pct Recovery = 120%  Analysis Date = 07/28/14 
 Pct Recovery = 120%  Analysis Date = 07/24/14 
 Pct Recovery = 120%  Analysis Date = 07/24/14 
 Pct Recovery = 120%  Analysis Date = 07/20/14 
 Pct Recovery = 120%  Analysis Date = 07/20/14 
 Pct Recovery = 120%  Analysis Date = 07/16/14 
 Pct Recovery = 120%  Analysis Date = 07/16/14 
 Pct Recovery = 120%  Analysis Date = 07/11/14 
 Pct Recovery = 120%  Analysis Date = 07/11/14 
 Pct Recovery = 120%  Analysis Date = 07/07/14 
 Pct Recovery = 120%  Analysis Date = 07/07/14 
 Pct Recovery = 120%  Analysis Date = 07/03/14 
 Pct Recovery = 120%  Analysis Date = 07/03/14 
 Pct Recovery = 120%  Analysis Date = 06/29/14 
 Pct Recovery = 120%  Analysis Date = 06/29/14 
 Pct Recovery = 120%  Analysis Date = 06/25/14 
 Pct Recovery = 120%  Analysis Date = 06/25/14 
 Pct Recovery = 120%  Analysis Date = 06/21/14 
 Pct Recovery = 120%  Analysis Date = 06/21/14 
 Pct Recovery = 120%  Analysis Date = 06/17/14 
 Pct Recovery = 120%  Analysis Date = 06/17/14 
 Pct Recovery = 120%  Analysis Date = 06/13/14 
 Pct Recovery = 120%  Analysis Date = 06/13/14 
 Pct Recovery = 120%  Analysis Date = 06/09/14 
 Pct Recovery = 120%  Analysis Date = 06/09/14 
 Pct Recovery = 120%  Analysis Date = 06/05/14 
 Pct Recovery = 120%  Analysis Date = 06/05/14 
 Pct Recovery = 120%  Analysis Date = 06/01/14 
 Pct Recovery = 121%  Analysis Date = 06/01/14 
 Pct Recovery = 121%  Analysis Date = 05/28/14 
 Pct Recovery = 121%  Analysis Date = 05/28/14 
 Pct Recovery = 121%  Analysis Date = 05/24/14 
 Pct Recovery = 121%  Analysis Date = 05/24/14 
 Pct Recovery = 121%  Analysis Date = 05/20/14 
 Pct Recovery = 121%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
TERT-BUTYL METHYL ETHER (MTBE)

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 32 116% 22% 111% 23%
Total 32 116% 22% 111% 23%

Sample Statistics
TERT-BUTYL METHYL ETHER (MTBE)

Characteristic N % % Basis
Plotted 32 89% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 3 8% Spiked
Spiked 36 .  
False Negatives 1 3% 1 out of 36
Not Spiked 17 .  
False Positives 1 6% 1 out of 17

BQS OBSP Determination:
TRANS-CROTONALDEHYDE
METHOD: 4437 , TESTIDCODE: 68733GM016
Open Data Set

 Analysis Date = 01/10/15 
 SpikeMix = Abs 032014: 20 µl & ERA 0321-14-05A: 20 µl 
 Pct Recovery = 117%  Analysis Date = 08/13/14 
 SpikeMix = ERA 0321-14-05: 20 µl & Accu 214031128: 20 µl 
 Pct Recovery = 117%  Analysis Date = 07/11/14 
 SpikeMix = ChemService 2615700: 20 µl & Accu 214031128: 20 µl 
 Pct Recovery = 46%  Analysis Date = 07/03/14 
 SpikeMix = Abs 032014: 20 µl & ChemService 2615700: 20 µl 
 Pct Recovery = 47%  Analysis Date = 06/07/14 
 SpikeMix = ChemService 2615700: 20 µl & Supelco LC06437: 20 µl 
 Pct Recovery = 49%  Analysis Date = 06/06/14 
 SpikeMix = NSI 031814: 20 µl & ChemService 2615700: 20 µl 
 Pct Recovery = 46%  Analysis Date = 10/09/15 
 SpikeMix = Supelco LC13544: 25 µl & NSI 050515HVOC: 25 µl 
 Pct Recovery = 92%  Analysis Date = 10/09/15 
 SpikeMix = ERA 0601-15-05: 25 µl & Accu 215041338: 25 µl 
 Pct Recovery = 88%  Analysis Date = 06/26/15 
 SpikeMix = ChemService 3818700: 25 µl & Accu 215041338: 25 µl 
 Pct Recovery = 78%  Analysis Date = 08/12/16 
 SpikeMix = Accu 216041354: 15 µl & Abs 060916HVOC: 15 µl 
 Pct Recovery = 101%  Analysis Date = 04/28/16 
 SpikeMix = ChemService 3818700: 15 µl & Supelco LC13544: 15 µl 
 Pct Recovery = 82%  Analysis Date = 08/24/15 
 SpikeMix = ERA 0601-15-05: 15 µl & Supelco LC13544: 15 µl 
 Pct Recovery = 75%  Analysis Date = 07/30/15 
 SpikeMix = Supelco LC13544: 15 µl & NSI 050515HVOC: 15 µl 
 Pct Recovery = 72%  Analysis Date = 05/14/15 
 SpikeMix = ChemService 3818700: 15 µl & Supelco LC13544: 15 µl 
 Pct Recovery = 141%  Analysis Date = 11/25/15 
 SpikeMix = Accu 215041338: 15 µl & Abs 040315: 15 µl 
 Pct Recovery = 76%  Analysis Date = 09/05/15 
 SpikeMix = Accu 215041338: 15 µl & NSI 050515HVOC: 15 µl 
 Pct Recovery = 84%  Analysis Date = 04/25/15 
 SpikeMix = Abs 032014: 10 µl & ERA 0321-14-05A: 10 µl 
 Pct Recovery = 146%  Analysis Date = 10/21/14 
 SpikeMix = ERA 0321-14-05A: 10 µl & Accu 214031128: 10 µl 
 Pct Recovery = 124%  Analysis Date = 09/06/14 
 SpikeMix = ERA 0321-14-05: 10 µl & Supelco LC06437: 10 µl 
 Pct Recovery = 132%  Analysis Date = 11/22/14 
 SpikeMix = ChemService 2615700: 10 µl & Supelco LC06437: 10 µl 
 Pct Recovery = 50%  Analysis Date = 07/30/14 
 SpikeMix = NSI 031814: 10 µl & ChemService 2615700: 10 µl 
 Pct Recovery = 43%  Analysis Date = 05/20/14 
 SpikeMix = ChemService 2615700: 10 µl & Accu 214031128: 10 µl 
 Pct Recovery = 44%  Analysis Date = 03/22/16 
 SpikeMix = Supelco LC13544: 10 µl & NSI 050515HVOC: 10 µl 
 Pct Recovery = 95%  Analysis Date = 12/10/15 
 SpikeMix = ChemService 3818700: 10 µl & Supelco LC13544: 10 µl 
 Pct Recovery = 80%  Analysis Date = 05/05/15 
 SpikeMix = Supelco LC13544: 10 µl & Abs 040315: 10 µl 
 Pct Recovery = 135%  Analysis Date = 02/12/16 
 SpikeMix = ERA 0601-15-05: 10 µl & Accu 215041338: 10 µl 
 Pct Recovery = 77%  Analysis Date = 01/05/16 
 SpikeMix = Accu 215041338: 10 µl & Abs 040315: 10 µl 
 Pct Recovery = 63%  Analysis Date = 05/20/15 
 SpikeMix = ChemService 3818700: 10 µl & Accu 215041338: 10 µl 
 Pct Recovery = 110%  Analysis Date = 08/12/16 
 Pct Recovery = 95%  Analysis Date = 08/07/16 
 Pct Recovery = 95%  Analysis Date = 08/07/16 
 Pct Recovery = 95%  Analysis Date = 08/03/16 
 Pct Recovery = 94%  Analysis Date = 08/03/16 
 Pct Recovery = 94%  Analysis Date = 07/30/16 
 Pct Recovery = 94%  Analysis Date = 07/30/16 
 Pct Recovery = 94%  Analysis Date = 07/26/16 
 Pct Recovery = 94%  Analysis Date = 07/26/16 
 Pct Recovery = 94%  Analysis Date = 07/22/16 
 Pct Recovery = 94%  Analysis Date = 07/22/16 
 Pct Recovery = 94%  Analysis Date = 07/18/16 
 Pct Recovery = 93%  Analysis Date = 07/18/16 
 Pct Recovery = 93%  Analysis Date = 07/14/16 
 Pct Recovery = 93%  Analysis Date = 07/14/16 
 Pct Recovery = 93%  Analysis Date = 07/10/16 
 Pct Recovery = 93%  Analysis Date = 07/10/16 
 Pct Recovery = 93%  Analysis Date = 07/06/16 
 Pct Recovery = 93%  Analysis Date = 07/06/16 
 Pct Recovery = 93%  Analysis Date = 07/02/16 
 Pct Recovery = 92%  Analysis Date = 07/02/16 
 Pct Recovery = 92%  Analysis Date = 06/28/16 
 Pct Recovery = 92%  Analysis Date = 06/28/16 
 Pct Recovery = 92%  Analysis Date = 06/24/16 
 Pct Recovery = 92%  Analysis Date = 06/24/16 
 Pct Recovery = 92%  Analysis Date = 06/20/16 
 Pct Recovery = 92%  Analysis Date = 06/20/16 
 Pct Recovery = 92%  Analysis Date = 06/15/16 
 Pct Recovery = 91%  Analysis Date = 06/15/16 
 Pct Recovery = 91%  Analysis Date = 06/11/16 
 Pct Recovery = 91%  Analysis Date = 06/11/16 
 Pct Recovery = 91%  Analysis Date = 06/07/16 
 Pct Recovery = 91%  Analysis Date = 06/07/16 
 Pct Recovery = 91%  Analysis Date = 06/03/16 
 Pct Recovery = 91%  Analysis Date = 06/03/16 
 Pct Recovery = 91%  Analysis Date = 05/30/16 
 Pct Recovery = 90%  Analysis Date = 05/30/16 
 Pct Recovery = 90%  Analysis Date = 05/26/16 
 Pct Recovery = 90%  Analysis Date = 05/26/16 
 Pct Recovery = 90%  Analysis Date = 05/22/16 
 Pct Recovery = 90%  Analysis Date = 05/22/16 
 Pct Recovery = 90%  Analysis Date = 05/18/16 
 Pct Recovery = 89%  Analysis Date = 05/18/16 
 Pct Recovery = 89%  Analysis Date = 05/14/16 
 Pct Recovery = 89%  Analysis Date = 05/14/16 
 Pct Recovery = 89%  Analysis Date = 05/10/16 
 Pct Recovery = 89%  Analysis Date = 05/10/16 
 Pct Recovery = 89%  Analysis Date = 05/06/16 
 Pct Recovery = 89%  Analysis Date = 05/06/16 
 Pct Recovery = 89%  Analysis Date = 05/02/16 
 Pct Recovery = 88%  Analysis Date = 05/02/16 
 Pct Recovery = 88%  Analysis Date = 04/28/16 
 Pct Recovery = 88%  Analysis Date = 04/28/16 
 Pct Recovery = 88%  Analysis Date = 04/23/16 
 Pct Recovery = 88%  Analysis Date = 04/23/16 
 Pct Recovery = 88%  Analysis Date = 04/19/16 
 Pct Recovery = 88%  Analysis Date = 04/19/16 
 Pct Recovery = 88%  Analysis Date = 04/15/16 
 Pct Recovery = 87%  Analysis Date = 04/15/16 
 Pct Recovery = 87%  Analysis Date = 04/11/16 
 Pct Recovery = 87%  Analysis Date = 04/11/16 
 Pct Recovery = 87%  Analysis Date = 04/07/16 
 Pct Recovery = 87%  Analysis Date = 04/07/16 
 Pct Recovery = 87%  Analysis Date = 04/03/16 
 Pct Recovery = 87%  Analysis Date = 04/03/16 
 Pct Recovery = 87%  Analysis Date = 03/30/16 
 Pct Recovery = 86%  Analysis Date = 03/30/16 
 Pct Recovery = 86%  Analysis Date = 03/26/16 
 Pct Recovery = 86%  Analysis Date = 03/26/16 
 Pct Recovery = 86%  Analysis Date = 03/22/16 
 Pct Recovery = 86%  Analysis Date = 03/22/16 
 Pct Recovery = 86%  Analysis Date = 03/18/16 
 Pct Recovery = 85%  Analysis Date = 03/18/16 
 Pct Recovery = 85%  Analysis Date = 03/14/16 
 Pct Recovery = 85%  Analysis Date = 03/14/16 
 Pct Recovery = 85%  Analysis Date = 03/10/16 
 Pct Recovery = 85%  Analysis Date = 03/10/16 
 Pct Recovery = 85%  Analysis Date = 03/06/16 
 Pct Recovery = 85%  Analysis Date = 03/06/16 
 Pct Recovery = 85%  Analysis Date = 03/02/16 
 Pct Recovery = 84%  Analysis Date = 03/02/16 
 Pct Recovery = 84%  Analysis Date = 02/26/16 
 Pct Recovery = 84%  Analysis Date = 02/26/16 
 Pct Recovery = 84%  Analysis Date = 02/22/16 
 Pct Recovery = 84%  Analysis Date = 02/22/16 
 Pct Recovery = 84%  Analysis Date = 02/18/16 
 Pct Recovery = 84%  Analysis Date = 02/18/16 
 Pct Recovery = 84%  Analysis Date = 02/14/16 
 Pct Recovery = 83%  Analysis Date = 02/14/16 
 Pct Recovery = 83%  Analysis Date = 02/10/16 
 Pct Recovery = 83%  Analysis Date = 02/10/16 
 Pct Recovery = 83%  Analysis Date = 02/06/16 
 Pct Recovery = 83%  Analysis Date = 02/06/16 
 Pct Recovery = 83%  Analysis Date = 02/02/16 
 Pct Recovery = 83%  Analysis Date = 02/02/16 
 Pct Recovery = 83%  Analysis Date = 01/29/16 
 Pct Recovery = 83%  Analysis Date = 01/29/16 
 Pct Recovery = 83%  Analysis Date = 01/25/16 
 Pct Recovery = 82%  Analysis Date = 01/25/16 
 Pct Recovery = 82%  Analysis Date = 01/21/16 
 Pct Recovery = 82%  Analysis Date = 01/21/16 
 Pct Recovery = 82%  Analysis Date = 01/17/16 
 Pct Recovery = 82%  Analysis Date = 01/17/16 
 Pct Recovery = 82%  Analysis Date = 01/13/16 
 Pct Recovery = 82%  Analysis Date = 01/13/16 
 Pct Recovery = 82%  Analysis Date = 01/09/16 
 Pct Recovery = 82%  Analysis Date = 01/09/16 
 Pct Recovery = 82%  Analysis Date = 01/04/16 
 Pct Recovery = 82%  Analysis Date = 01/04/16 
 Pct Recovery = 82%  Analysis Date = 12/31/15 
 Pct Recovery = 81%  Analysis Date = 12/31/15 
 Pct Recovery = 81%  Analysis Date = 12/27/15 
 Pct Recovery = 81%  Analysis Date = 12/27/15 
 Pct Recovery = 81%  Analysis Date = 12/23/15 
 Pct Recovery = 81%  Analysis Date = 12/23/15 
 Pct Recovery = 81%  Analysis Date = 12/19/15 
 Pct Recovery = 81%  Analysis Date = 12/19/15 
 Pct Recovery = 81%  Analysis Date = 12/15/15 
 Pct Recovery = 81%  Analysis Date = 12/15/15 
 Pct Recovery = 81%  Analysis Date = 12/11/15 
 Pct Recovery = 81%  Analysis Date = 12/11/15 
 Pct Recovery = 81%  Analysis Date = 12/07/15 
 Pct Recovery = 81%  Analysis Date = 12/07/15 
 Pct Recovery = 81%  Analysis Date = 12/03/15 
 Pct Recovery = 81%  Analysis Date = 12/03/15 
 Pct Recovery = 81%  Analysis Date = 11/29/15 
 Pct Recovery = 81%  Analysis Date = 11/29/15 
 Pct Recovery = 81%  Analysis Date = 11/25/15 
 Pct Recovery = 81%  Analysis Date = 11/25/15 
 Pct Recovery = 81%  Analysis Date = 11/21/15 
 Pct Recovery = 81%  Analysis Date = 11/21/15 
 Pct Recovery = 81%  Analysis Date = 11/17/15 
 Pct Recovery = 81%  Analysis Date = 11/17/15 
 Pct Recovery = 81%  Analysis Date = 11/12/15 
 Pct Recovery = 81%  Analysis Date = 11/12/15 
 Pct Recovery = 81%  Analysis Date = 11/08/15 
 Pct Recovery = 81%  Analysis Date = 11/08/15 
 Pct Recovery = 81%  Analysis Date = 11/04/15 
 Pct Recovery = 82%  Analysis Date = 11/04/15 
 Pct Recovery = 82%  Analysis Date = 10/31/15 
 Pct Recovery = 82%  Analysis Date = 10/31/15 
 Pct Recovery = 82%  Analysis Date = 10/27/15 
 Pct Recovery = 82%  Analysis Date = 10/27/15 
 Pct Recovery = 82%  Analysis Date = 10/23/15 
 Pct Recovery = 82%  Analysis Date = 10/23/15 
 Pct Recovery = 82%  Analysis Date = 10/19/15 
 Pct Recovery = 82%  Analysis Date = 10/19/15 
 Pct Recovery = 82%  Analysis Date = 10/15/15 
 Pct Recovery = 82%  Analysis Date = 10/15/15 
 Pct Recovery = 82%  Analysis Date = 10/11/15 
 Pct Recovery = 82%  Analysis Date = 10/11/15 
 Pct Recovery = 82%  Analysis Date = 10/07/15 
 Pct Recovery = 83%  Analysis Date = 10/07/15 
 Pct Recovery = 83%  Analysis Date = 10/03/15 
 Pct Recovery = 84%  Analysis Date = 10/03/15 
 Pct Recovery = 84%  Analysis Date = 09/29/15 
 Pct Recovery = 85%  Analysis Date = 09/29/15 
 Pct Recovery = 85%  Analysis Date = 09/25/15 
 Pct Recovery = 85%  Analysis Date = 09/25/15 
 Pct Recovery = 85%  Analysis Date = 09/21/15 
 Pct Recovery = 86%  Analysis Date = 09/21/15 
 Pct Recovery = 86%  Analysis Date = 09/16/15 
 Pct Recovery = 87%  Analysis Date = 09/16/15 
 Pct Recovery = 87%  Analysis Date = 09/12/15 
 Pct Recovery = 88%  Analysis Date = 09/12/15 
 Pct Recovery = 88%  Analysis Date = 09/08/15 
 Pct Recovery = 89%  Analysis Date = 09/08/15 
 Pct Recovery = 89%  Analysis Date = 09/04/15 
 Pct Recovery = 90%  Analysis Date = 09/04/15 
 Pct Recovery = 90%  Analysis Date = 08/31/15 
 Pct Recovery = 91%  Analysis Date = 08/31/15 
 Pct Recovery = 91%  Analysis Date = 08/27/15 
 Pct Recovery = 92%  Analysis Date = 08/27/15 
 Pct Recovery = 92%  Analysis Date = 08/23/15 
 Pct Recovery = 93%  Analysis Date = 08/23/15 
 Pct Recovery = 93%  Analysis Date = 08/19/15 
 Pct Recovery = 94%  Analysis Date = 08/19/15 
 Pct Recovery = 94%  Analysis Date = 08/15/15 
 Pct Recovery = 95%  Analysis Date = 08/15/15 
 Pct Recovery = 95%  Analysis Date = 08/11/15 
 Pct Recovery = 96%  Analysis Date = 08/11/15 
 Pct Recovery = 96%  Analysis Date = 08/07/15 
 Pct Recovery = 96%  Analysis Date = 08/07/15 
 Pct Recovery = 96%  Analysis Date = 08/03/15 
 Pct Recovery = 97%  Analysis Date = 08/03/15 
 Pct Recovery = 97%  Analysis Date = 07/30/15 
 Pct Recovery = 98%  Analysis Date = 07/30/15 
 Pct Recovery = 98%  Analysis Date = 07/25/15 
 Pct Recovery = 99%  Analysis Date = 07/25/15 
 Pct Recovery = 99%  Analysis Date = 07/21/15 
 Pct Recovery = 100%  Analysis Date = 07/21/15 
 Pct Recovery = 100%  Analysis Date = 07/17/15 
 Pct Recovery = 101%  Analysis Date = 07/17/15 
 Pct Recovery = 101%  Analysis Date = 07/13/15 
 Pct Recovery = 102%  Analysis Date = 07/13/15 
 Pct Recovery = 102%  Analysis Date = 07/09/15 
 Pct Recovery = 103%  Analysis Date = 07/09/15 
 Pct Recovery = 103%  Analysis Date = 07/05/15 
 Pct Recovery = 104%  Analysis Date = 07/05/15 
 Pct Recovery = 104%  Analysis Date = 07/01/15 
 Pct Recovery = 105%  Analysis Date = 07/01/15 
 Pct Recovery = 105%  Analysis Date = 06/27/15 
 Pct Recovery = 106%  Analysis Date = 06/27/15 
 Pct Recovery = 106%  Analysis Date = 06/23/15 
 Pct Recovery = 106%  Analysis Date = 06/23/15 
 Pct Recovery = 106%  Analysis Date = 06/19/15 
 Pct Recovery = 107%  Analysis Date = 06/19/15 
 Pct Recovery = 107%  Analysis Date = 06/15/15 
 Pct Recovery = 107%  Analysis Date = 06/15/15 
 Pct Recovery = 107%  Analysis Date = 06/11/15 
 Pct Recovery = 108%  Analysis Date = 06/11/15 
 Pct Recovery = 108%  Analysis Date = 06/07/15 
 Pct Recovery = 108%  Analysis Date = 06/07/15 
 Pct Recovery = 108%  Analysis Date = 06/02/15 
 Pct Recovery = 108%  Analysis Date = 06/02/15 
 Pct Recovery = 108%  Analysis Date = 05/29/15 
 Pct Recovery = 109%  Analysis Date = 05/29/15 
 Pct Recovery = 109%  Analysis Date = 05/25/15 
 Pct Recovery = 109%  Analysis Date = 05/25/15 
 Pct Recovery = 109%  Analysis Date = 05/21/15 
 Pct Recovery = 109%  Analysis Date = 05/21/15 
 Pct Recovery = 109%  Analysis Date = 05/17/15 
 Pct Recovery = 110%  Analysis Date = 05/17/15 
 Pct Recovery = 110%  Analysis Date = 05/13/15 
 Pct Recovery = 110%  Analysis Date = 05/13/15 
 Pct Recovery = 110%  Analysis Date = 05/09/15 
 Pct Recovery = 110%  Analysis Date = 05/09/15 
 Pct Recovery = 110%  Analysis Date = 05/05/15 
 Pct Recovery = 110%  Analysis Date = 05/05/15 
 Pct Recovery = 110%  Analysis Date = 05/01/15 
 Pct Recovery = 110%  Analysis Date = 05/01/15 
 Pct Recovery = 110%  Analysis Date = 04/27/15 
 Pct Recovery = 110%  Analysis Date = 04/27/15 
 Pct Recovery = 110%  Analysis Date = 04/23/15 
 Pct Recovery = 110%  Analysis Date = 04/23/15 
 Pct Recovery = 110%  Analysis Date = 04/19/15 
 Pct Recovery = 110%  Analysis Date = 04/19/15 
 Pct Recovery = 110%  Analysis Date = 04/15/15 
 Pct Recovery = 110%  Analysis Date = 04/15/15 
 Pct Recovery = 110%  Analysis Date = 04/11/15 
 Pct Recovery = 110%  Analysis Date = 04/11/15 
 Pct Recovery = 110%  Analysis Date = 04/06/15 
 Pct Recovery = 110%  Analysis Date = 04/06/15 
 Pct Recovery = 110%  Analysis Date = 04/02/15 
 Pct Recovery = 110%  Analysis Date = 04/02/15 
 Pct Recovery = 110%  Analysis Date = 03/29/15 
 Pct Recovery = 110%  Analysis Date = 03/29/15 
 Pct Recovery = 110%  Analysis Date = 03/25/15 
 Pct Recovery = 110%  Analysis Date = 03/25/15 
 Pct Recovery = 110%  Analysis Date = 03/21/15 
 Pct Recovery = 110%  Analysis Date = 03/21/15 
 Pct Recovery = 110%  Analysis Date = 03/17/15 
 Pct Recovery = 110%  Analysis Date = 03/17/15 
 Pct Recovery = 110%  Analysis Date = 03/13/15 
 Pct Recovery = 110%  Analysis Date = 03/13/15 
 Pct Recovery = 110%  Analysis Date = 03/09/15 
 Pct Recovery = 110%  Analysis Date = 03/09/15 
 Pct Recovery = 110%  Analysis Date = 03/05/15 
 Pct Recovery = 110%  Analysis Date = 03/05/15 
 Pct Recovery = 110%  Analysis Date = 03/01/15 
 Pct Recovery = 110%  Analysis Date = 03/01/15 
 Pct Recovery = 110%  Analysis Date = 02/25/15 
 Pct Recovery = 110%  Analysis Date = 02/25/15 
 Pct Recovery = 110%  Analysis Date = 02/21/15 
 Pct Recovery = 110%  Analysis Date = 02/21/15 
 Pct Recovery = 110%  Analysis Date = 02/17/15 
 Pct Recovery = 110%  Analysis Date = 02/17/15 
 Pct Recovery = 110%  Analysis Date = 02/12/15 
 Pct Recovery = 110%  Analysis Date = 02/12/15 
 Pct Recovery = 110%  Analysis Date = 02/08/15 
 Pct Recovery = 110%  Analysis Date = 02/08/15 
 Pct Recovery = 110%  Analysis Date = 02/04/15 
 Pct Recovery = 110%  Analysis Date = 02/04/15 
 Pct Recovery = 110%  Analysis Date = 01/31/15 
 Pct Recovery = 110%  Analysis Date = 01/31/15 
 Pct Recovery = 110%  Analysis Date = 01/27/15 
 Pct Recovery = 110%  Analysis Date = 01/27/15 
 Pct Recovery = 110%  Analysis Date = 01/23/15 
 Pct Recovery = 111%  Analysis Date = 01/23/15 
 Pct Recovery = 111%  Analysis Date = 01/19/15 
 Pct Recovery = 111%  Analysis Date = 01/19/15 
 Pct Recovery = 111%  Analysis Date = 01/15/15 
 Pct Recovery = 111%  Analysis Date = 01/15/15 
 Pct Recovery = 111%  Analysis Date = 01/11/15 
 Pct Recovery = 111%  Analysis Date = 01/11/15 
 Pct Recovery = 111%  Analysis Date = 01/07/15 
 Pct Recovery = 110%  Analysis Date = 01/07/15 
 Pct Recovery = 110%  Analysis Date = 01/03/15 
 Pct Recovery = 109%  Analysis Date = 01/03/15 
 Pct Recovery = 109%  Analysis Date = 12/30/14 
 Pct Recovery = 108%  Analysis Date = 12/30/14 
 Pct Recovery = 108%  Analysis Date = 12/26/14 
 Pct Recovery = 107%  Analysis Date = 12/26/14 
 Pct Recovery = 107%  Analysis Date = 12/21/14 
 Pct Recovery = 106%  Analysis Date = 12/21/14 
 Pct Recovery = 106%  Analysis Date = 12/17/14 
 Pct Recovery = 106%  Analysis Date = 12/17/14 
 Pct Recovery = 106%  Analysis Date = 12/13/14 
 Pct Recovery = 105%  Analysis Date = 12/13/14 
 Pct Recovery = 105%  Analysis Date = 12/09/14 
 Pct Recovery = 104%  Analysis Date = 12/09/14 
 Pct Recovery = 104%  Analysis Date = 12/05/14 
 Pct Recovery = 103%  Analysis Date = 12/05/14 
 Pct Recovery = 103%  Analysis Date = 12/01/14 
 Pct Recovery = 102%  Analysis Date = 12/01/14 
 Pct Recovery = 102%  Analysis Date = 11/27/14 
 Pct Recovery = 101%  Analysis Date = 11/27/14 
 Pct Recovery = 101%  Analysis Date = 11/23/14 
 Pct Recovery = 100%  Analysis Date = 11/23/14 
 Pct Recovery = 100%  Analysis Date = 11/19/14 
 Pct Recovery = 99%  Analysis Date = 11/19/14 
 Pct Recovery = 99%  Analysis Date = 11/15/14 
 Pct Recovery = 98%  Analysis Date = 11/15/14 
 Pct Recovery = 98%  Analysis Date = 11/11/14 
 Pct Recovery = 98%  Analysis Date = 11/11/14 
 Pct Recovery = 98%  Analysis Date = 11/07/14 
 Pct Recovery = 97%  Analysis Date = 11/07/14 
 Pct Recovery = 97%  Analysis Date = 11/03/14 
 Pct Recovery = 96%  Analysis Date = 11/03/14 
 Pct Recovery = 96%  Analysis Date = 10/30/14 
 Pct Recovery = 95%  Analysis Date = 10/30/14 
 Pct Recovery = 95%  Analysis Date = 10/25/14 
 Pct Recovery = 94%  Analysis Date = 10/25/14 
 Pct Recovery = 94%  Analysis Date = 10/21/14 
 Pct Recovery = 93%  Analysis Date = 10/21/14 
 Pct Recovery = 93%  Analysis Date = 10/17/14 
 Pct Recovery = 92%  Analysis Date = 10/17/14 
 Pct Recovery = 92%  Analysis Date = 10/13/14 
 Pct Recovery = 91%  Analysis Date = 10/13/14 
 Pct Recovery = 91%  Analysis Date = 10/09/14 
 Pct Recovery = 90%  Analysis Date = 10/09/14 
 Pct Recovery = 90%  Analysis Date = 10/05/14 
 Pct Recovery = 89%  Analysis Date = 10/05/14 
 Pct Recovery = 89%  Analysis Date = 10/01/14 
 Pct Recovery = 87%  Analysis Date = 10/01/14 
 Pct Recovery = 87%  Analysis Date = 09/27/14 
 Pct Recovery = 86%  Analysis Date = 09/27/14 
 Pct Recovery = 86%  Analysis Date = 09/23/14 
 Pct Recovery = 85%  Analysis Date = 09/23/14 
 Pct Recovery = 85%  Analysis Date = 09/19/14 
 Pct Recovery = 84%  Analysis Date = 09/19/14 
 Pct Recovery = 84%  Analysis Date = 09/15/14 
 Pct Recovery = 83%  Analysis Date = 09/15/14 
 Pct Recovery = 83%  Analysis Date = 09/11/14 
 Pct Recovery = 82%  Analysis Date = 09/11/14 
 Pct Recovery = 82%  Analysis Date = 09/07/14 
 Pct Recovery = 80%  Analysis Date = 09/07/14 
 Pct Recovery = 80%  Analysis Date = 09/02/14 
 Pct Recovery = 79%  Analysis Date = 09/02/14 
 Pct Recovery = 79%  Analysis Date = 08/29/14 
 Pct Recovery = 78%  Analysis Date = 08/29/14 
 Pct Recovery = 78%  Analysis Date = 08/25/14 
 Pct Recovery = 77%  Analysis Date = 08/25/14 
 Pct Recovery = 77%  Analysis Date = 08/21/14 
 Pct Recovery = 76%  Analysis Date = 08/21/14 
 Pct Recovery = 76%  Analysis Date = 08/17/14 
 Pct Recovery = 75%  Analysis Date = 08/17/14 
 Pct Recovery = 75%  Analysis Date = 08/13/14 
 Pct Recovery = 73%  Analysis Date = 08/13/14 
 Pct Recovery = 73%  Analysis Date = 08/09/14 
 Pct Recovery = 72%  Analysis Date = 08/09/14 
 Pct Recovery = 72%  Analysis Date = 08/05/14 
 Pct Recovery = 71%  Analysis Date = 08/05/14 
 Pct Recovery = 71%  Analysis Date = 08/01/14 
 Pct Recovery = 70%  Analysis Date = 08/01/14 
 Pct Recovery = 70%  Analysis Date = 07/28/14 
 Pct Recovery = 68%  Analysis Date = 07/28/14 
 Pct Recovery = 68%  Analysis Date = 07/24/14 
 Pct Recovery = 67%  Analysis Date = 07/24/14 
 Pct Recovery = 67%  Analysis Date = 07/20/14 
 Pct Recovery = 66%  Analysis Date = 07/20/14 
 Pct Recovery = 66%  Analysis Date = 07/16/14 
 Pct Recovery = 65%  Analysis Date = 07/16/14 
 Pct Recovery = 65%  Analysis Date = 07/11/14 
 Pct Recovery = 64%  Analysis Date = 07/11/14 
 Pct Recovery = 64%  Analysis Date = 07/07/14 
 Pct Recovery = 62%  Analysis Date = 07/07/14 
 Pct Recovery = 62%  Analysis Date = 07/03/14 
 Pct Recovery = 61%  Analysis Date = 07/03/14 
 Pct Recovery = 61%  Analysis Date = 06/29/14 
 Pct Recovery = 60%  Analysis Date = 06/29/14 
 Pct Recovery = 60%  Analysis Date = 06/25/14 
 Pct Recovery = 58%  Analysis Date = 06/25/14 
 Pct Recovery = 58%  Analysis Date = 06/21/14 
 Pct Recovery = 57%  Analysis Date = 06/21/14 
 Pct Recovery = 57%  Analysis Date = 06/17/14 
 Pct Recovery = 56%  Analysis Date = 06/17/14 
 Pct Recovery = 56%  Analysis Date = 06/13/14 
 Pct Recovery = 55%  Analysis Date = 06/13/14 
 Pct Recovery = 55%  Analysis Date = 06/09/14 
 Pct Recovery = 53%  Analysis Date = 06/09/14 
 Pct Recovery = 53%  Analysis Date = 06/05/14 
 Pct Recovery = 52%  Analysis Date = 06/05/14 
 Pct Recovery = 52%  Analysis Date = 06/01/14 
 Pct Recovery = 51%  Analysis Date = 06/01/14 
 Pct Recovery = 51%  Analysis Date = 05/28/14 
 Pct Recovery = 49%  Analysis Date = 05/28/14 
 Pct Recovery = 49%  Analysis Date = 05/24/14 
 Pct Recovery = 48%  Analysis Date = 05/24/14 
 Pct Recovery = 48%  Analysis Date = 05/20/14 
 Pct Recovery = 47%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
TRANS-CROTONALDEHYDE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 28 86% 32% 81% 42%
Total 28 86% 32% 81% 42%

Sample Statistics
TRANS-CROTONALDEHYDE

Characteristic N % % Basis
Plotted 28 100% Spiked
Estimated Values 4 14% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 28 .  
False Negatives 0 0% 0 out of 28
Not Spiked 20 .  
False Positives 0 0% 0 out of 20