BQS OBSP Determination:
11-KETOTESTOSTERONE
METHOD: 4434 , TESTIDCODE: 64527GM005
Open Data Set

Analysis Date = 12/03/12 SpikeMix = ERA 0511-12-02: 50 µl & Abs 051512: 50 µl Pct Recovery = 97% Analysis Date = 11/07/12 SpikeMix = ERA 0507-12-04.1: 50 µl & ERA 0511-12-02: 50 µl Pct Recovery = 98% Analysis Date = 08/31/12 SpikeMix = ERA 0511-12-02: 25 µl & Abs 051512: 25 µl Pct Recovery = 95% Analysis Date = 04/10/13 SpikeMix = ERA 0511-12-02: 25 µl & Supelco LB92781: 25 µl Pct Recovery = 102% Analysis Date = 04/03/13 SpikeMix = Spex Organics T1120525010: 25 µl & Abs 051512: 25 µl Pct Recovery = 74% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120525010: 25 µl & ERA 0511-12-02: 25 µl Pct Recovery = 108% Analysis Date = 11/01/12 SpikeMix = ERA 0507-12-04.1: 25 µl & Abs 051512: 25 µl Pct Recovery = 77% Analysis Date = 08/24/12 SpikeMix = Abs 051512: 25 µl Pct Recovery = 108% Analysis Date = 03/14/14 SpikeMix = Supelco LB99393: 50 µl & Abs 050813: 50 µl Pct Recovery = 111% Analysis Date = 03/14/14 SpikeMix = Supelco LB99393: 50 µl & Abs 060413: 50 µl & Abs 071513: 50 µl Pct Recovery = 88% Analysis Date = 03/05/14 SpikeMix = ERA 0415-13-01.1A: 50 µl & Abs 060413: 50 µl & Abs 071513: 50 µl Pct Recovery = 93% Analysis Date = 02/25/14 SpikeMix = ERA 0415-13-01.1A: 50 µl & Abs 050813: 50 µl Pct Recovery = 84% Analysis Date = 04/01/15 SpikeMix = Spex Organics E1140505004: 60 µl & Supelco LC06946: 60 µl Pct Recovery = 102% Analysis Date = 02/12/15 SpikeMix = Supelco LC06946: 60 µl & Abs 042114: 60 µl Pct Recovery = 78% Analysis Date = 12/09/14 SpikeMix = Abs 031014: 60 µl & Supelco LC06946: 60 µl Pct Recovery = 88% Analysis Date = 09/23/14 SpikeMix = Supelco LC06946: 60 µl & ChemService 2561700: 60 µl Pct Recovery = 88% Analysis Date = 01/07/16 SpikeMix = Crescent 04EE007: 60 µl & Abs 041515: 60 µl Pct Recovery = 96% Analysis Date = 02/01/17 SpikeMix = Supelco LC20140V: 30 µl & Abs 052616: 30 µl Pct Recovery = 90% Analysis Date = 01/13/17 SpikeMix = Abs 052616: 30 µl & ChemService 5016200: 30 µl Pct Recovery = 82% Analysis Date = 12/29/16 SpikeMix = ChemService 5016100: 30 µl & Abs 052616: 30 µl Pct Recovery = 106% Analysis Date = 12/05/16 SpikeMix = Abs 052616: 30 µl & Abs 061416H: 30 µl Pct Recovery = 106% Analysis Date = 06/24/16 SpikeMix = Crescent 04EE007: 50 µl & Spex Organics EN150501025: 50 µl Pct Recovery = 53% Analysis Date = 01/08/16 SpikeMix = Crescent 04EE007: 50 µl & Spex Organics EN150501025: 50 µl Pct Recovery = 91% Analysis Date = 08/10/15 SpikeMix = ERA 0601-15-04: 50 µl & Crescent 04EE007: 50 µl Pct Recovery = 102% Analysis Date = 01/29/15 SpikeMix = Abs 031014: 30 µl & Supelco LC06946: 30 µl Pct Recovery = 70% Analysis Date = 01/21/15 SpikeMix = Supelco LC06946: 30 µl & ChemService 2561700: 30 µl Pct Recovery = 82% Analysis Date = 12/23/14 SpikeMix = Spex Organics E1140505004: 30 µl & Supelco LC06946: 30 µl Pct Recovery = 69% Analysis Date = 12/16/14 SpikeMix = Supelco LC06946: 30 µl & Abs 042114: 30 µl Pct Recovery = 78% Analysis Date = 03/03/14 SpikeMix = Abs 050813: 20 µl & Abs 071513: 20 µl Pct Recovery = 86% Analysis Date = 01/23/14 SpikeMix = Supelco LB99393: 20 µl & ERA 0415-13-01.2A: 20 µl & Abs 060413: 20 µl Pct Recovery = 95% Analysis Date = 11/18/13 SpikeMix = ERA 0415-13-01.2A: 20 µl & Abs 050813: 20 µl Pct Recovery = 106% Analysis Date = 09/16/13 SpikeMix = ERA 0415-13-01.1A: 20 µl & ERA 0415-13-01.2A: 20 µl & Abs 060413: 20 µl Pct Recovery = 123% Analysis Date = 01/08/16 SpikeMix = ERA 0601-15-04: 30 µl & Crescent 04EE007: 30 µl Pct Recovery = 128% Analysis Date = 11/02/15 SpikeMix = Supelco LC13547: 30 µl & Crescent 04EE007: 30 µl Pct Recovery = 88% Analysis Date = 02/01/17 Pct Recovery = 94% Analysis Date = 01/23/17 Pct Recovery = 94% Analysis Date = 01/23/17 Pct Recovery = 94% Analysis Date = 01/15/17 Pct Recovery = 94% Analysis Date = 01/15/17 Pct Recovery = 94% Analysis Date = 01/07/17 Pct Recovery = 94% Analysis Date = 01/07/17 Pct Recovery = 94% Analysis Date = 12/30/16 Pct Recovery = 94% Analysis Date = 12/30/16 Pct Recovery = 94% Analysis Date = 12/22/16 Pct Recovery = 94% Analysis Date = 12/22/16 Pct Recovery = 94% Analysis Date = 12/14/16 Pct Recovery = 94% Analysis Date = 12/14/16 Pct Recovery = 94% Analysis Date = 12/06/16 Pct Recovery = 93% Analysis Date = 12/06/16 Pct Recovery = 93% Analysis Date = 11/28/16 Pct Recovery = 93% Analysis Date = 11/28/16 Pct Recovery = 93% Analysis Date = 11/20/16 Pct Recovery = 93% Analysis Date = 11/20/16 Pct Recovery = 93% Analysis Date = 11/11/16 Pct Recovery = 93% Analysis Date = 11/11/16 Pct Recovery = 93% Analysis Date = 11/03/16 Pct Recovery = 93% Analysis Date = 11/03/16 Pct Recovery = 93% Analysis Date = 10/26/16 Pct Recovery = 93% Analysis Date = 10/26/16 Pct Recovery = 93% Analysis Date = 10/18/16 Pct Recovery = 93% Analysis Date = 10/18/16 Pct Recovery = 93% Analysis Date = 10/10/16 Pct Recovery = 93% Analysis Date = 10/10/16 Pct Recovery = 93% Analysis Date = 10/02/16 Pct Recovery = 93% Analysis Date = 10/02/16 Pct Recovery = 93% Analysis Date = 09/24/16 Pct Recovery = 93% Analysis Date = 09/24/16 Pct Recovery = 93% Analysis Date = 09/16/16 Pct Recovery = 93% Analysis Date = 09/16/16 Pct Recovery = 93% Analysis Date = 09/08/16 Pct Recovery = 93% Analysis Date = 09/08/16 Pct Recovery = 93% Analysis Date = 08/30/16 Pct Recovery = 93% Analysis Date = 08/30/16 Pct Recovery = 93% Analysis Date = 08/22/16 Pct Recovery = 93% Analysis Date = 08/22/16 Pct Recovery = 93% Analysis Date = 08/14/16 Pct Recovery = 93% Analysis Date = 08/14/16 Pct Recovery = 93% Analysis Date = 08/06/16 Pct Recovery = 93% Analysis Date = 08/06/16 Pct Recovery = 93% Analysis Date = 07/29/16 Pct Recovery = 93% Analysis Date = 07/29/16 Pct Recovery = 93% Analysis Date = 07/21/16 Pct Recovery = 93% Analysis Date = 07/21/16 Pct Recovery = 93% Analysis Date = 07/13/16 Pct Recovery = 93% Analysis Date = 07/13/16 Pct Recovery = 93% Analysis Date = 07/05/16 Pct Recovery = 93% Analysis Date = 07/05/16 Pct Recovery = 93% Analysis Date = 06/27/16 Pct Recovery = 93% Analysis Date = 06/27/16 Pct Recovery = 93% Analysis Date = 06/18/16 Pct Recovery = 92% Analysis Date = 06/18/16 Pct Recovery = 92% Analysis Date = 06/10/16 Pct Recovery = 92% Analysis Date = 06/10/16 Pct Recovery = 92% Analysis Date = 06/02/16 Pct Recovery = 92% Analysis Date = 06/02/16 Pct Recovery = 92% Analysis Date = 05/25/16 Pct Recovery = 92% Analysis Date = 05/25/16 Pct Recovery = 92% Analysis Date = 05/17/16 Pct Recovery = 92% Analysis Date = 05/17/16 Pct Recovery = 92% Analysis Date = 05/09/16 Pct Recovery = 92% Analysis Date = 05/09/16 Pct Recovery = 92% Analysis Date = 05/01/16 Pct Recovery = 92% Analysis Date = 05/01/16 Pct Recovery = 92% Analysis Date = 04/23/16 Pct Recovery = 92% Analysis Date = 04/23/16 Pct Recovery = 92% Analysis Date = 04/15/16 Pct Recovery = 92% Analysis Date = 04/15/16 Pct Recovery = 92% Analysis Date = 04/06/16 Pct Recovery = 92% Analysis Date = 04/06/16 Pct Recovery = 92% Analysis Date = 03/29/16 Pct Recovery = 92% Analysis Date = 03/29/16 Pct Recovery = 92% Analysis Date = 03/21/16 Pct Recovery = 92% Analysis Date = 03/21/16 Pct Recovery = 92% Analysis Date = 03/13/16 Pct Recovery = 92% Analysis Date = 03/13/16 Pct Recovery = 92% Analysis Date = 03/05/16 Pct Recovery = 91% Analysis Date = 03/05/16 Pct Recovery = 91% Analysis Date = 02/26/16 Pct Recovery = 91% Analysis Date = 02/26/16 Pct Recovery = 91% Analysis Date = 02/18/16 Pct Recovery = 91% Analysis Date = 02/18/16 Pct Recovery = 91% Analysis Date = 02/10/16 Pct Recovery = 91% Analysis Date = 02/10/16 Pct Recovery = 91% Analysis Date = 02/02/16 Pct Recovery = 91% Analysis Date = 02/02/16 Pct Recovery = 91% Analysis Date = 01/24/16 Pct Recovery = 91% Analysis Date = 01/24/16 Pct Recovery = 91% Analysis Date = 01/16/16 Pct Recovery = 91% Analysis Date = 01/16/16 Pct Recovery = 91% Analysis Date = 01/08/16 Pct Recovery = 91% Analysis Date = 01/08/16 Pct Recovery = 91% Analysis Date = 12/31/15 Pct Recovery = 91% Analysis Date = 12/31/15 Pct Recovery = 91% Analysis Date = 12/23/15 Pct Recovery = 91% Analysis Date = 12/23/15 Pct Recovery = 91% Analysis Date = 12/15/15 Pct Recovery = 91% Analysis Date = 12/15/15 Pct Recovery = 91% Analysis Date = 12/07/15 Pct Recovery = 91% Analysis Date = 12/07/15 Pct Recovery = 91% Analysis Date = 11/29/15 Pct Recovery = 90% Analysis Date = 11/29/15 Pct Recovery = 90% Analysis Date = 11/21/15 Pct Recovery = 90% Analysis Date = 11/21/15 Pct Recovery = 90% Analysis Date = 11/12/15 Pct Recovery = 90% Analysis Date = 11/12/15 Pct Recovery = 90% Analysis Date = 11/04/15 Pct Recovery = 90% Analysis Date = 11/04/15 Pct Recovery = 90% Analysis Date = 10/27/15 Pct Recovery = 90% Analysis Date = 10/27/15 Pct Recovery = 90% Analysis Date = 10/19/15 Pct Recovery = 90% Analysis Date = 10/19/15 Pct Recovery = 90% Analysis Date = 10/11/15 Pct Recovery = 90% Analysis Date = 10/11/15 Pct Recovery = 90% Analysis Date = 10/03/15 Pct Recovery = 90% Analysis Date = 10/03/15 Pct Recovery = 90% Analysis Date = 09/25/15 Pct Recovery = 90% Analysis Date = 09/25/15 Pct Recovery = 90% Analysis Date = 09/17/15 Pct Recovery = 89% Analysis Date = 09/17/15 Pct Recovery = 89% Analysis Date = 09/09/15 Pct Recovery = 89% Analysis Date = 09/09/15 Pct Recovery = 89% Analysis Date = 08/31/15 Pct Recovery = 89% Analysis Date = 08/31/15 Pct Recovery = 89% Analysis Date = 08/23/15 Pct Recovery = 89% Analysis Date = 08/23/15 Pct Recovery = 89% Analysis Date = 08/15/15 Pct Recovery = 89% Analysis Date = 08/15/15 Pct Recovery = 89% Analysis Date = 08/07/15 Pct Recovery = 89% Analysis Date = 08/07/15 Pct Recovery = 89% Analysis Date = 07/30/15 Pct Recovery = 89% Analysis Date = 07/30/15 Pct Recovery = 89% Analysis Date = 07/22/15 Pct Recovery = 89% Analysis Date = 07/22/15 Pct Recovery = 89% Analysis Date = 07/14/15 Pct Recovery = 88% Analysis Date = 07/14/15 Pct Recovery = 88% Analysis Date = 07/06/15 Pct Recovery = 88% Analysis Date = 07/06/15 Pct Recovery = 88% Analysis Date = 06/28/15 Pct Recovery = 88% Analysis Date = 06/28/15 Pct Recovery = 88% Analysis Date = 06/19/15 Pct Recovery = 88% Analysis Date = 06/19/15 Pct Recovery = 88% Analysis Date = 06/11/15 Pct Recovery = 88% Analysis Date = 06/11/15 Pct Recovery = 88% Analysis Date = 06/03/15 Pct Recovery = 88% Analysis Date = 06/03/15 Pct Recovery = 88% Analysis Date = 05/26/15 Pct Recovery = 88% Analysis Date = 05/26/15 Pct Recovery = 88% Analysis Date = 05/18/15 Pct Recovery = 88% Analysis Date = 05/18/15 Pct Recovery = 88% Analysis Date = 05/10/15 Pct Recovery = 87% Analysis Date = 05/10/15 Pct Recovery = 87% Analysis Date = 05/02/15 Pct Recovery = 87% Analysis Date = 05/02/15 Pct Recovery = 87% Analysis Date = 04/24/15 Pct Recovery = 87% Analysis Date = 04/24/15 Pct Recovery = 87% Analysis Date = 04/16/15 Pct Recovery = 87% Analysis Date = 04/16/15 Pct Recovery = 87% Analysis Date = 04/07/15 Pct Recovery = 87% Analysis Date = 04/07/15 Pct Recovery = 87% Analysis Date = 03/30/15 Pct Recovery = 87% Analysis Date = 03/30/15 Pct Recovery = 87% Analysis Date = 03/22/15 Pct Recovery = 87% Analysis Date = 03/22/15 Pct Recovery = 87% Analysis Date = 03/14/15 Pct Recovery = 86% Analysis Date = 03/14/15 Pct Recovery = 86% Analysis Date = 03/06/15 Pct Recovery = 86% Analysis Date = 03/06/15 Pct Recovery = 86% Analysis Date = 02/26/15 Pct Recovery = 86% Analysis Date = 02/26/15 Pct Recovery = 86% Analysis Date = 02/18/15 Pct Recovery = 86% Analysis Date = 02/18/15 Pct Recovery = 86% Analysis Date = 02/10/15 Pct Recovery = 86% Analysis Date = 02/10/15 Pct Recovery = 86% Analysis Date = 02/02/15 Pct Recovery = 86% Analysis Date = 02/02/15 Pct Recovery = 86% Analysis Date = 01/24/15 Pct Recovery = 86% Analysis Date = 01/24/15 Pct Recovery = 86% Analysis Date = 01/16/15 Pct Recovery = 85% Analysis Date = 01/16/15 Pct Recovery = 85% Analysis Date = 01/08/15 Pct Recovery = 85% Analysis Date = 01/08/15 Pct Recovery = 85% Analysis Date = 12/31/14 Pct Recovery = 85% Analysis Date = 12/31/14 Pct Recovery = 85% Analysis Date = 12/23/14 Pct Recovery = 84% Analysis Date = 12/23/14 Pct Recovery = 84% Analysis Date = 12/15/14 Pct Recovery = 85% Analysis Date = 12/15/14 Pct Recovery = 85% Analysis Date = 12/07/14 Pct Recovery = 85% Analysis Date = 12/07/14 Pct Recovery = 85% Analysis Date = 11/29/14 Pct Recovery = 85% Analysis Date = 11/29/14 Pct Recovery = 85% Analysis Date = 11/21/14 Pct Recovery = 85% Analysis Date = 11/21/14 Pct Recovery = 85% Analysis Date = 11/13/14 Pct Recovery = 85% Analysis Date = 11/13/14 Pct Recovery = 85% Analysis Date = 11/04/14 Pct Recovery = 86% Analysis Date = 11/04/14 Pct Recovery = 86% Analysis Date = 10/27/14 Pct Recovery = 86% Analysis Date = 10/27/14 Pct Recovery = 86% Analysis Date = 10/19/14 Pct Recovery = 86% Analysis Date = 10/19/14 Pct Recovery = 86% Analysis Date = 10/11/14 Pct Recovery = 86% Analysis Date = 10/11/14 Pct Recovery = 86% Analysis Date = 10/03/14 Pct Recovery = 86% Analysis Date = 10/03/14 Pct Recovery = 86% Analysis Date = 09/25/14 Pct Recovery = 87% Analysis Date = 09/25/14 Pct Recovery = 87% Analysis Date = 09/17/14 Pct Recovery = 87% Analysis Date = 09/17/14 Pct Recovery = 87% Analysis Date = 09/09/14 Pct Recovery = 87% Analysis Date = 09/09/14 Pct Recovery = 87% Analysis Date = 09/01/14 Pct Recovery = 88% Analysis Date = 09/01/14 Pct Recovery = 88% Analysis Date = 08/23/14 Pct Recovery = 88% Analysis Date = 08/23/14 Pct Recovery = 88% Analysis Date = 08/15/14 Pct Recovery = 88% Analysis Date = 08/15/14 Pct Recovery = 88% Analysis Date = 08/07/14 Pct Recovery = 89% Analysis Date = 08/07/14 Pct Recovery = 89% Analysis Date = 07/30/14 Pct Recovery = 89% Analysis Date = 07/30/14 Pct Recovery = 89% Analysis Date = 07/22/14 Pct Recovery = 89% Analysis Date = 07/22/14 Pct Recovery = 89% Analysis Date = 07/14/14 Pct Recovery = 90% Analysis Date = 07/14/14 Pct Recovery = 90% Analysis Date = 07/06/14 Pct Recovery = 90% Analysis Date = 07/06/14 Pct Recovery = 90% Analysis Date = 06/28/14 Pct Recovery = 90% Analysis Date = 06/28/14 Pct Recovery = 90% Analysis Date = 06/20/14 Pct Recovery = 91% Analysis Date = 06/20/14 Pct Recovery = 91% Analysis Date = 06/11/14 Pct Recovery = 91% Analysis Date = 06/11/14 Pct Recovery = 91% Analysis Date = 06/03/14 Pct Recovery = 91% Analysis Date = 06/03/14 Pct Recovery = 91% Analysis Date = 05/26/14 Pct Recovery = 91% Analysis Date = 05/26/14 Pct Recovery = 91% Analysis Date = 05/18/14 Pct Recovery = 92% Analysis Date = 05/18/14 Pct Recovery = 92% Analysis Date = 05/10/14 Pct Recovery = 92% Analysis Date = 05/10/14 Pct Recovery = 92% Analysis Date = 05/02/14 Pct Recovery = 92% Analysis Date = 05/02/14 Pct Recovery = 92% Analysis Date = 04/24/14 Pct Recovery = 93% Analysis Date = 04/24/14 Pct Recovery = 93% Analysis Date = 04/16/14 Pct Recovery = 93% Analysis Date = 04/16/14 Pct Recovery = 93% Analysis Date = 04/08/14 Pct Recovery = 93% Analysis Date = 04/08/14 Pct Recovery = 93% Analysis Date = 03/30/14 Pct Recovery = 94% Analysis Date = 03/30/14 Pct Recovery = 94% Analysis Date = 03/22/14 Pct Recovery = 94% Analysis Date = 03/22/14 Pct Recovery = 94% Analysis Date = 03/14/14 Pct Recovery = 94% Analysis Date = 03/14/14 Pct Recovery = 94% Analysis Date = 03/06/14 Pct Recovery = 95% Analysis Date = 03/06/14 Pct Recovery = 95% Analysis Date = 02/26/14 Pct Recovery = 95% Analysis Date = 02/26/14 Pct Recovery = 95% Analysis Date = 02/18/14 Pct Recovery = 95% Analysis Date = 02/18/14 Pct Recovery = 95% Analysis Date = 02/10/14 Pct Recovery = 95% Analysis Date = 02/10/14 Pct Recovery = 95% Analysis Date = 02/02/14 Pct Recovery = 95% Analysis Date = 02/02/14 Pct Recovery = 95% Analysis Date = 01/25/14 Pct Recovery = 95% Analysis Date = 01/25/14 Pct Recovery = 95% Analysis Date = 01/16/14 Pct Recovery = 95% Analysis Date = 01/16/14 Pct Recovery = 95% Analysis Date = 01/08/14 Pct Recovery = 96% Analysis Date = 01/08/14 Pct Recovery = 96% Analysis Date = 12/31/13 Pct Recovery = 96% Analysis Date = 12/31/13 Pct Recovery = 96% Analysis Date = 12/23/13 Pct Recovery = 96% Analysis Date = 12/23/13 Pct Recovery = 96% Analysis Date = 12/15/13 Pct Recovery = 96% Analysis Date = 12/15/13 Pct Recovery = 96% Analysis Date = 12/07/13 Pct Recovery = 96% Analysis Date = 12/07/13 Pct Recovery = 96% Analysis Date = 11/29/13 Pct Recovery = 96% Analysis Date = 11/29/13 Pct Recovery = 96% Analysis Date = 11/21/13 Pct Recovery = 96% Analysis Date = 11/21/13 Pct Recovery = 96% Analysis Date = 11/13/13 Pct Recovery = 96% Analysis Date = 11/13/13 Pct Recovery = 96% Analysis Date = 11/04/13 Pct Recovery = 96% Analysis Date = 11/04/13 Pct Recovery = 96% Analysis Date = 10/27/13 Pct Recovery = 97% Analysis Date = 10/27/13 Pct Recovery = 97% Analysis Date = 10/19/13 Pct Recovery = 97% Analysis Date = 10/19/13 Pct Recovery = 97% Analysis Date = 10/11/13 Pct Recovery = 97% Analysis Date = 10/11/13 Pct Recovery = 97% Analysis Date = 10/03/13 Pct Recovery = 97% Analysis Date = 10/03/13 Pct Recovery = 97% Analysis Date = 09/25/13 Pct Recovery = 97% Analysis Date = 09/25/13 Pct Recovery = 97% Analysis Date = 09/17/13 Pct Recovery = 97% Analysis Date = 09/17/13 Pct Recovery = 97% Analysis Date = 09/09/13 Pct Recovery = 97% Analysis Date = 09/09/13 Pct Recovery = 97% Analysis Date = 09/01/13 Pct Recovery = 97% Analysis Date = 09/01/13 Pct Recovery = 97% Analysis Date = 08/23/13 Pct Recovery = 97% Analysis Date = 08/23/13 Pct Recovery = 97% Analysis Date = 08/15/13 Pct Recovery = 97% Analysis Date = 08/15/13 Pct Recovery = 97% Analysis Date = 08/07/13 Pct Recovery = 97% Analysis Date = 08/07/13 Pct Recovery = 97% Analysis Date = 07/30/13 Pct Recovery = 97% Analysis Date = 07/30/13 Pct Recovery = 97% Analysis Date = 07/22/13 Pct Recovery = 97% Analysis Date = 07/22/13 Pct Recovery = 97% Analysis Date = 07/14/13 Pct Recovery = 97% Analysis Date = 07/14/13 Pct Recovery = 97% Analysis Date = 07/06/13 Pct Recovery = 97% Analysis Date = 07/06/13 Pct Recovery = 97% Analysis Date = 06/28/13 Pct Recovery = 97% Analysis Date = 06/28/13 Pct Recovery = 97% Analysis Date = 06/20/13 Pct Recovery = 97% Analysis Date = 06/20/13 Pct Recovery = 97% Analysis Date = 06/11/13 Pct Recovery = 97% Analysis Date = 06/11/13 Pct Recovery = 97% Analysis Date = 06/03/13 Pct Recovery = 97% Analysis Date = 06/03/13 Pct Recovery = 97% Analysis Date = 05/26/13 Pct Recovery = 97% Analysis Date = 05/26/13 Pct Recovery = 97% Analysis Date = 05/18/13 Pct Recovery = 97% Analysis Date = 05/18/13 Pct Recovery = 97% Analysis Date = 05/10/13 Pct Recovery = 97% Analysis Date = 05/10/13 Pct Recovery = 97% Analysis Date = 05/02/13 Pct Recovery = 97% Analysis Date = 05/02/13 Pct Recovery = 97% Analysis Date = 04/24/13 Pct Recovery = 97% Analysis Date = 04/24/13 Pct Recovery = 97% Analysis Date = 04/16/13 Pct Recovery = 97% Analysis Date = 04/16/13 Pct Recovery = 97% Analysis Date = 04/08/13 Pct Recovery = 97% Analysis Date = 04/08/13 Pct Recovery = 97% Analysis Date = 03/30/13 Pct Recovery = 97% Analysis Date = 03/30/13 Pct Recovery = 97% Analysis Date = 03/22/13 Pct Recovery = 97% Analysis Date = 03/22/13 Pct Recovery = 97% Analysis Date = 03/14/13 Pct Recovery = 97% Analysis Date = 03/14/13 Pct Recovery = 97% Analysis Date = 03/06/13 Pct Recovery = 97% Analysis Date = 03/06/13 Pct Recovery = 97% Analysis Date = 02/26/13 Pct Recovery = 97% Analysis Date = 02/26/13 Pct Recovery = 97% Analysis Date = 02/18/13 Pct Recovery = 97% Analysis Date = 02/18/13 Pct Recovery = 97% Analysis Date = 02/10/13 Pct Recovery = 97% Analysis Date = 02/10/13 Pct Recovery = 97% Analysis Date = 02/02/13 Pct Recovery = 97% Analysis Date = 02/02/13 Pct Recovery = 97% Analysis Date = 01/25/13 Pct Recovery = 97% Analysis Date = 01/25/13 Pct Recovery = 97% Analysis Date = 01/16/13 Pct Recovery = 97% Analysis Date = 01/16/13 Pct Recovery = 97% Analysis Date = 01/08/13 Pct Recovery = 97% Analysis Date = 01/08/13 Pct Recovery = 97% Analysis Date = 12/31/12 Pct Recovery = 97% Analysis Date = 12/31/12 Pct Recovery = 97% Analysis Date = 12/23/12 Pct Recovery = 97% Analysis Date = 12/23/12 Pct Recovery = 97% Analysis Date = 12/15/12 Pct Recovery = 97% Analysis Date = 12/15/12 Pct Recovery = 97% Analysis Date = 12/07/12 Pct Recovery = 97% Analysis Date = 12/07/12 Pct Recovery = 97% Analysis Date = 11/29/12 Pct Recovery = 97% Analysis Date = 11/29/12 Pct Recovery = 97% Analysis Date = 11/21/12 Pct Recovery = 97% Analysis Date = 11/21/12 Pct Recovery = 97% Analysis Date = 11/13/12 Pct Recovery = 97% Analysis Date = 11/13/12 Pct Recovery = 97% Analysis Date = 11/04/12 Pct Recovery = 96% Analysis Date = 11/04/12 Pct Recovery = 96% Analysis Date = 10/27/12 Pct Recovery = 96% Analysis Date = 10/27/12 Pct Recovery = 96% Analysis Date = 10/19/12 Pct Recovery = 96% Analysis Date = 10/19/12 Pct Recovery = 96% Analysis Date = 10/11/12 Pct Recovery = 96% Analysis Date = 10/11/12 Pct Recovery = 96% Analysis Date = 10/03/12 Pct Recovery = 96% Analysis Date = 10/03/12 Pct Recovery = 96% Analysis Date = 09/25/12 Pct Recovery = 96% Analysis Date = 09/25/12 Pct Recovery = 96% Analysis Date = 09/17/12 Pct Recovery = 96% Analysis Date = 09/17/12 Pct Recovery = 96% Analysis Date = 09/09/12 Pct Recovery = 96% Analysis Date = 09/09/12 Pct Recovery = 96% Analysis Date = 09/01/12 Pct Recovery = 96% Analysis Date = 09/01/12 Pct Recovery = 96% Analysis Date = 08/24/12 Pct Recovery = 96% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
11-KETOTESTOSTERONE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 34 92% 16% 92% 15%
Total 34 92% 16% 92% 15%

Sample Statistics
11-KETOTESTOSTERONE

Characteristic N % % Basis
Plotted 34 89% Spiked
Estimated Values 0 0% Spiked
Deleted Values 2 2% Spiked + Not Spiked
Spiked, Censored 1 3% Spiked
Spiked 39 .  
False Negatives 3 8% 3 out of 38
Not Spiked 92 .  
False Positives 0 0% 0 out of 91

BQS OBSP Determination:
17-ALPHA-ESTRADIOL
METHOD: 4434 , TESTIDCODE: 64528GM005
Open Data Set

Analysis Date = 08/19/16 SpikeMix = Supelco LC20140V: 50 µl & Spex Organics TS160420010: 50 µl Pct Recovery = 251% Analysis Date = 03/27/12 SpikeMix = Crescent 162776: 100 µl Pct Recovery = 92% Analysis Date = 01/27/12 SpikeMix = Supelco LB77167: 100 µl Pct Recovery = 79% Analysis Date = 10/13/11 SpikeMix = Supelco LB77167: 100 µl Pct Recovery = 89% Analysis Date = 06/07/11 SpikeMix = Supelco LB77167: 100 µl Pct Recovery = 91% Analysis Date = 03/10/11 SpikeMix = Crescent 162776: 100 µl Pct Recovery = 89% Analysis Date = 06/23/11 SpikeMix = Crescent 162776: 100 µl Pct Recovery = 93% Analysis Date = 03/14/14 SpikeMix = Supelco LB99393: 50 µl & Abs 050813: 50 µl Pct Recovery = 82% Analysis Date = 03/14/14 SpikeMix = Supelco LB99393: 50 µl & Abs 060413: 50 µl & Abs 071513: 50 µl Pct Recovery = 67% Analysis Date = 04/14/14 SpikeMix = ERA 0415-13-01.1A: 50 µl & Abs 071513: 50 µl Pct Recovery = 92% Analysis Date = 03/05/14 SpikeMix = ERA 0415-13-01.1A: 50 µl & Abs 060413: 50 µl & Abs 071513: 50 µl Pct Recovery = 84% Analysis Date = 02/25/14 SpikeMix = ERA 0415-13-01.1A: 50 µl & Abs 050813: 50 µl Pct Recovery = 70% Analysis Date = 12/15/16 SpikeMix = Abs 061416H: 50 µl & ChemService 5016100: 50 µl Pct Recovery = 100% Analysis Date = 08/11/16 SpikeMix = ChemService 5016100: 50 µl & Spex Organics TS160420010: 50 µl Pct Recovery = 170% Analysis Date = 04/22/13 SpikeMix = ERA 0507-12-04.1: 50 µl & Restek A089631: 50 µl Pct Recovery = 77% Analysis Date = 12/18/12 SpikeMix = ERA 0507-12-04.1: 50 µl & Restek A089631: 50 µl Pct Recovery = 75% Analysis Date = 11/07/12 SpikeMix = ERA 0507-12-04.1: 50 µl & ERA 0511-12-02: 50 µl Pct Recovery = 88% Analysis Date = 04/13/15 SpikeMix = Abs 042114: 60 µl & Spex Organics E1140505004: 60 µl Pct Recovery = 69% Analysis Date = 04/01/15 SpikeMix = Spex Organics E1140505004: 60 µl & Supelco LC06946: 60 µl Pct Recovery = 97% Analysis Date = 01/21/15 SpikeMix = ChemService 2561700: 60 µl & Spex Organics E1140505004: 60 µl Pct Recovery = 86% Analysis Date = 12/09/14 SpikeMix = Abs 031014: 60 µl & Supelco LC06946: 60 µl Pct Recovery = 88% Analysis Date = 08/26/14 SpikeMix = Abs 031014: 60 µl & Abs 042114: 60 µl Pct Recovery = 92% Analysis Date = 05/06/14 SpikeMix = Abs 031014: 60 µl & ChemService 2561700: 60 µl Pct Recovery = 127% Analysis Date = 04/03/13 SpikeMix = Spex Organics T1120525010: 50 µl & Restek A089631: 50 µl Pct Recovery = 89% Analysis Date = 12/18/12 SpikeMix = Spex Organics T1120525010: 50 µl & Supelco LB92781: 50 µl Pct Recovery = 88% Analysis Date = 01/07/16 SpikeMix = Crescent 04EE007: 60 µl & Abs 041515: 60 µl Pct Recovery = 76% Analysis Date = 01/08/16 SpikeMix = Spex Organics EN150501025: 60 µl & ERA 0601-15-04: 60 µl Pct Recovery = 102% Analysis Date = 07/27/12 SpikeMix = Supelco LB77167: 25 µl Pct Recovery = 80% Analysis Date = 04/17/12 SpikeMix = Supelco LB77167: 25 µl Pct Recovery = 108% Analysis Date = 04/06/12 SpikeMix = Crescent 162776: 25 µl Pct Recovery = 111% Analysis Date = 04/04/12 SpikeMix = Supelco LB77167: 25 µl Pct Recovery = 102% Analysis Date = 11/17/11 SpikeMix = Crescent 162776: 25 µl Pct Recovery = 85% Analysis Date = 10/12/11 SpikeMix = Crescent 162776: 25 µl Pct Recovery = 88% Analysis Date = 09/29/11 SpikeMix = Supelco LB77167: 25 µl Pct Recovery = 70% Analysis Date = 07/25/11 SpikeMix = Crescent 162776: 25 µl Pct Recovery = 53% Analysis Date = 05/19/11 SpikeMix = Supelco LB77167: 25 µl Pct Recovery = 98% Analysis Date = 03/31/11 SpikeMix = Supelco LB77167: 25 µl Pct Recovery = 76% Analysis Date = 05/09/11 SpikeMix = Crescent 162776: 25 µl Pct Recovery = 71% Analysis Date = 02/01/17 SpikeMix = Supelco LC20140V: 30 µl & Abs 052616: 30 µl Pct Recovery = 90% Analysis Date = 09/15/16 SpikeMix = Supelco LC20140V: 30 µl & Spex Organics EN160621015: 30 µl Pct Recovery = 88% Analysis Date = 09/09/16 SpikeMix = ChemService 5016200: 30 µl & Supelco LC20140V: 30 µl Pct Recovery = 104% Analysis Date = 01/23/14 SpikeMix = Supelco LB99393: 20 µl & ERA 0415-13-01.2A: 20 µl & Abs 060413: 20 µl Pct Recovery = 70% Analysis Date = 12/09/13 SpikeMix = Supelco LB99393: 20 µl & Spex Organics T1130423008: 20 µl Pct Recovery = 66% Analysis Date = 07/19/13 SpikeMix = Supelco LB99393: 20 µl & ERA 0415-13-01.2A: 20 µl Pct Recovery = 81% Analysis Date = 06/04/13 SpikeMix = Supelco LB99393: 20 µl & Spex Organics T1130423008: 20 µl Pct Recovery = 75% Analysis Date = 03/07/16 SpikeMix = Abs 041515: 50 µl & ERA 0601-15-04: 50 µl Pct Recovery = 54% Analysis Date = 12/10/15 SpikeMix = Abs 041515: 50 µl & ERA 0601-15-04: 50 µl Pct Recovery = 75% Analysis Date = 08/17/15 SpikeMix = ChemService 4073900: 50 µl & Abs 041515: 50 µl Pct Recovery = 87% Analysis Date = 06/24/16 SpikeMix = Crescent 04EE007: 50 µl & Spex Organics EN150501025: 50 µl Pct Recovery = 100% Analysis Date = 01/08/16 SpikeMix = Crescent 04EE007: 50 µl & Spex Organics EN150501025: 50 µl Pct Recovery = 84% Analysis Date = 04/14/14 SpikeMix = ERA 0415-13-01.1A: 20 µl & ERA 0415-13-01.2A: 20 µl & Abs 060413: 20 µl Pct Recovery = 90% Analysis Date = 09/16/13 SpikeMix = ERA 0415-13-01.1A: 20 µl & ERA 0415-13-01.2A: 20 µl & Abs 060413: 20 µl Pct Recovery = 94% Analysis Date = 06/27/13 SpikeMix = ERA 0415-13-01.1A: 20 µl & Spex Organics T1130423008: 20 µl Pct Recovery = 66% Analysis Date = 12/29/16 SpikeMix = ChemService 5016100: 30 µl & Abs 052616: 30 µl Pct Recovery = 93% Analysis Date = 09/21/16 SpikeMix = ChemService 5016200: 30 µl & ChemService 5016100: 30 µl Pct Recovery = 87% Analysis Date = 02/08/13 SpikeMix = ERA 0507-12-04.1: 25 µl & Supelco LB92781: 25 µl Pct Recovery = 78% Analysis Date = 11/01/12 SpikeMix = ERA 0507-12-04.1: 25 µl & Abs 051512: 25 µl Pct Recovery = 89% Analysis Date = 06/03/15 SpikeMix = Abs 031014: 30 µl & ERA 0227-14-07.2: 30 µl Pct Recovery = 105% Analysis Date = 04/01/15 SpikeMix = ChemService 2561700: 30 µl & Spex Organics E1140505004: 30 µl Pct Recovery = 83% Analysis Date = 01/29/15 SpikeMix = Abs 031014: 30 µl & Supelco LC06946: 30 µl Pct Recovery = 72% Analysis Date = 12/23/14 SpikeMix = Spex Organics E1140505004: 30 µl & Supelco LC06946: 30 µl Pct Recovery = 80% Analysis Date = 12/22/14 SpikeMix = Abs 042114: 30 µl & Abs 031014: 30 µl Pct Recovery = 93% Analysis Date = 09/04/14 SpikeMix = ERA 0227-14-07.2: 30 µl & Spex Organics E1140505004: 30 µl Pct Recovery = 75% Analysis Date = 07/14/14 SpikeMix = ERA 0227-14-07.2: 30 µl & Abs 031014: 30 µl Pct Recovery = 85% Analysis Date = 05/14/14 SpikeMix = Abs 031014: 30 µl & ChemService 2561700: 30 µl Pct Recovery = 93% Analysis Date = 04/03/13 SpikeMix = Spex Organics T1120525010: 25 µl & Abs 051512: 25 µl Pct Recovery = 73% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120525010: 25 µl & ERA 0511-12-02: 25 µl Pct Recovery = 95% Analysis Date = 08/29/12 SpikeMix = Spex Organics T1120525010: 25 µl Pct Recovery = 100% Analysis Date = 03/07/16 SpikeMix = ChemService 4073900: 30 µl & Abs 041515: 30 µl Pct Recovery = 91% Analysis Date = 03/18/16 SpikeMix = Spex Organics EN150501025: 30 µl & Supelco LC13547: 30 µl Pct Recovery = 80% Analysis Date = 12/11/15 SpikeMix = Crescent 04EE007: 30 µl & Spex Organics EN150501025: 30 µl Pct Recovery = 68% Analysis Date = 09/23/15 SpikeMix = ChemService 4073900: 30 µl & Spex Organics EN150501025: 30 µl Pct Recovery = 107% Analysis Date = 02/01/17 Pct Recovery = 112% Analysis Date = 01/21/17 Pct Recovery = 112% Analysis Date = 01/21/17 Pct Recovery = 112% Analysis Date = 01/10/17 Pct Recovery = 111% Analysis Date = 01/10/17 Pct Recovery = 111% Analysis Date = 12/30/16 Pct Recovery = 111% Analysis Date = 12/30/16 Pct Recovery = 111% Analysis Date = 12/19/16 Pct Recovery = 110% Analysis Date = 12/19/16 Pct Recovery = 110% Analysis Date = 12/09/16 Pct Recovery = 110% Analysis Date = 12/09/16 Pct Recovery = 110% Analysis Date = 11/28/16 Pct Recovery = 110% Analysis Date = 11/28/16 Pct Recovery = 110% Analysis Date = 11/17/16 Pct Recovery = 109% Analysis Date = 11/17/16 Pct Recovery = 109% Analysis Date = 11/06/16 Pct Recovery = 109% Analysis Date = 11/06/16 Pct Recovery = 109% Analysis Date = 10/27/16 Pct Recovery = 108% Analysis Date = 10/27/16 Pct Recovery = 108% Analysis Date = 10/16/16 Pct Recovery = 108% Analysis Date = 10/16/16 Pct Recovery = 108% Analysis Date = 10/05/16 Pct Recovery = 107% Analysis Date = 10/05/16 Pct Recovery = 107% Analysis Date = 09/24/16 Pct Recovery = 107% Analysis Date = 09/24/16 Pct Recovery = 107% Analysis Date = 09/13/16 Pct Recovery = 106% Analysis Date = 09/13/16 Pct Recovery = 106% Analysis Date = 09/03/16 Pct Recovery = 106% Analysis Date = 09/03/16 Pct Recovery = 106% Analysis Date = 08/23/16 Pct Recovery = 106% Analysis Date = 08/23/16 Pct Recovery = 106% Analysis Date = 08/12/16 Pct Recovery = 105% Analysis Date = 08/12/16 Pct Recovery = 105% Analysis Date = 08/01/16 Pct Recovery = 105% Analysis Date = 08/01/16 Pct Recovery = 105% Analysis Date = 07/22/16 Pct Recovery = 105% Analysis Date = 07/22/16 Pct Recovery = 105% Analysis Date = 07/11/16 Pct Recovery = 104% Analysis Date = 07/11/16 Pct Recovery = 104% Analysis Date = 06/30/16 Pct Recovery = 104% Analysis Date = 06/30/16 Pct Recovery = 104% Analysis Date = 06/19/16 Pct Recovery = 103% Analysis Date = 06/19/16 Pct Recovery = 103% Analysis Date = 06/08/16 Pct Recovery = 103% Analysis Date = 06/08/16 Pct Recovery = 103% Analysis Date = 05/29/16 Pct Recovery = 103% Analysis Date = 05/29/16 Pct Recovery = 103% Analysis Date = 05/18/16 Pct Recovery = 102% Analysis Date = 05/18/16 Pct Recovery = 102% Analysis Date = 05/07/16 Pct Recovery = 102% Analysis Date = 05/07/16 Pct Recovery = 102% Analysis Date = 04/26/16 Pct Recovery = 102% Analysis Date = 04/26/16 Pct Recovery = 102% Analysis Date = 04/16/16 Pct Recovery = 101% Analysis Date = 04/16/16 Pct Recovery = 101% Analysis Date = 04/05/16 Pct Recovery = 101% Analysis Date = 04/05/16 Pct Recovery = 101% Analysis Date = 03/25/16 Pct Recovery = 100% Analysis Date = 03/25/16 Pct Recovery = 100% Analysis Date = 03/14/16 Pct Recovery = 100% Analysis Date = 03/14/16 Pct Recovery = 100% Analysis Date = 03/03/16 Pct Recovery = 100% Analysis Date = 03/03/16 Pct Recovery = 100% Analysis Date = 02/22/16 Pct Recovery = 99% Analysis Date = 02/22/16 Pct Recovery = 99% Analysis Date = 02/11/16 Pct Recovery = 99% Analysis Date = 02/11/16 Pct Recovery = 99% Analysis Date = 01/31/16 Pct Recovery = 99% Analysis Date = 01/31/16 Pct Recovery = 99% Analysis Date = 01/20/16 Pct Recovery = 98% Analysis Date = 01/20/16 Pct Recovery = 98% Analysis Date = 01/10/16 Pct Recovery = 98% Analysis Date = 01/10/16 Pct Recovery = 98% Analysis Date = 12/30/15 Pct Recovery = 97% Analysis Date = 12/30/15 Pct Recovery = 97% Analysis Date = 12/19/15 Pct Recovery = 97% Analysis Date = 12/19/15 Pct Recovery = 97% Analysis Date = 12/08/15 Pct Recovery = 97% Analysis Date = 12/08/15 Pct Recovery = 97% Analysis Date = 11/28/15 Pct Recovery = 96% Analysis Date = 11/28/15 Pct Recovery = 96% Analysis Date = 11/17/15 Pct Recovery = 96% Analysis Date = 11/17/15 Pct Recovery = 96% Analysis Date = 11/06/15 Pct Recovery = 96% Analysis Date = 11/06/15 Pct Recovery = 96% Analysis Date = 10/26/15 Pct Recovery = 95% Analysis Date = 10/26/15 Pct Recovery = 95% Analysis Date = 10/15/15 Pct Recovery = 95% Analysis Date = 10/15/15 Pct Recovery = 95% Analysis Date = 10/05/15 Pct Recovery = 94% Analysis Date = 10/05/15 Pct Recovery = 94% Analysis Date = 09/24/15 Pct Recovery = 94% Analysis Date = 09/24/15 Pct Recovery = 94% Analysis Date = 09/13/15 Pct Recovery = 94% Analysis Date = 09/13/15 Pct Recovery = 94% Analysis Date = 09/02/15 Pct Recovery = 93% Analysis Date = 09/02/15 Pct Recovery = 93% Analysis Date = 08/23/15 Pct Recovery = 93% Analysis Date = 08/23/15 Pct Recovery = 93% Analysis Date = 08/12/15 Pct Recovery = 93% Analysis Date = 08/12/15 Pct Recovery = 93% Analysis Date = 08/01/15 Pct Recovery = 92% Analysis Date = 08/01/15 Pct Recovery = 92% Analysis Date = 07/21/15 Pct Recovery = 92% Analysis Date = 07/21/15 Pct Recovery = 92% Analysis Date = 07/10/15 Pct Recovery = 91% Analysis Date = 07/10/15 Pct Recovery = 91% Analysis Date = 06/30/15 Pct Recovery = 91% Analysis Date = 06/30/15 Pct Recovery = 91% Analysis Date = 06/19/15 Pct Recovery = 90% Analysis Date = 06/19/15 Pct Recovery = 90% Analysis Date = 06/08/15 Pct Recovery = 90% Analysis Date = 06/08/15 Pct Recovery = 90% Analysis Date = 05/28/15 Pct Recovery = 89% Analysis Date = 05/28/15 Pct Recovery = 89% Analysis Date = 05/18/15 Pct Recovery = 89% Analysis Date = 05/18/15 Pct Recovery = 89% Analysis Date = 05/07/15 Pct Recovery = 89% Analysis Date = 05/07/15 Pct Recovery = 89% Analysis Date = 04/26/15 Pct Recovery = 88% Analysis Date = 04/26/15 Pct Recovery = 88% Analysis Date = 04/15/15 Pct Recovery = 88% Analysis Date = 04/15/15 Pct Recovery = 88% Analysis Date = 04/04/15 Pct Recovery = 87% Analysis Date = 04/04/15 Pct Recovery = 87% Analysis Date = 03/25/15 Pct Recovery = 87% Analysis Date = 03/25/15 Pct Recovery = 87% Analysis Date = 03/14/15 Pct Recovery = 87% Analysis Date = 03/14/15 Pct Recovery = 87% Analysis Date = 03/03/15 Pct Recovery = 87% Analysis Date = 03/03/15 Pct Recovery = 87% Analysis Date = 02/20/15 Pct Recovery = 86% Analysis Date = 02/20/15 Pct Recovery = 86% Analysis Date = 02/10/15 Pct Recovery = 86% Analysis Date = 02/10/15 Pct Recovery = 86% Analysis Date = 01/30/15 Pct Recovery = 86% Analysis Date = 01/30/15 Pct Recovery = 86% Analysis Date = 01/19/15 Pct Recovery = 86% Analysis Date = 01/19/15 Pct Recovery = 86% Analysis Date = 01/08/15 Pct Recovery = 86% Analysis Date = 01/08/15 Pct Recovery = 86% Analysis Date = 12/28/14 Pct Recovery = 86% Analysis Date = 12/28/14 Pct Recovery = 86% Analysis Date = 12/18/14 Pct Recovery = 85% Analysis Date = 12/18/14 Pct Recovery = 85% Analysis Date = 12/07/14 Pct Recovery = 85% Analysis Date = 12/07/14 Pct Recovery = 85% Analysis Date = 11/26/14 Pct Recovery = 85% Analysis Date = 11/26/14 Pct Recovery = 85% Analysis Date = 11/15/14 Pct Recovery = 85% Analysis Date = 11/15/14 Pct Recovery = 85% Analysis Date = 11/05/14 Pct Recovery = 85% Analysis Date = 11/05/14 Pct Recovery = 85% Analysis Date = 10/25/14 Pct Recovery = 85% Analysis Date = 10/25/14 Pct Recovery = 85% Analysis Date = 10/14/14 Pct Recovery = 85% Analysis Date = 10/14/14 Pct Recovery = 85% Analysis Date = 10/03/14 Pct Recovery = 85% Analysis Date = 10/03/14 Pct Recovery = 85% Analysis Date = 09/23/14 Pct Recovery = 85% Analysis Date = 09/23/14 Pct Recovery = 85% Analysis Date = 09/12/14 Pct Recovery = 85% Analysis Date = 09/12/14 Pct Recovery = 85% Analysis Date = 09/01/14 Pct Recovery = 85% Analysis Date = 09/01/14 Pct Recovery = 85% Analysis Date = 08/21/14 Pct Recovery = 85% Analysis Date = 08/21/14 Pct Recovery = 85% Analysis Date = 08/10/14 Pct Recovery = 84% Analysis Date = 08/10/14 Pct Recovery = 84% Analysis Date = 07/31/14 Pct Recovery = 84% Analysis Date = 07/31/14 Pct Recovery = 84% Analysis Date = 07/20/14 Pct Recovery = 84% Analysis Date = 07/20/14 Pct Recovery = 84% Analysis Date = 07/09/14 Pct Recovery = 84% Analysis Date = 07/09/14 Pct Recovery = 84% Analysis Date = 06/28/14 Pct Recovery = 84% Analysis Date = 06/28/14 Pct Recovery = 84% Analysis Date = 06/18/14 Pct Recovery = 84% Analysis Date = 06/18/14 Pct Recovery = 84% Analysis Date = 06/07/14 Pct Recovery = 84% Analysis Date = 06/07/14 Pct Recovery = 84% Analysis Date = 05/27/14 Pct Recovery = 84% Analysis Date = 05/27/14 Pct Recovery = 84% Analysis Date = 05/16/14 Pct Recovery = 84% Analysis Date = 05/16/14 Pct Recovery = 84% Analysis Date = 05/05/14 Pct Recovery = 84% Analysis Date = 05/05/14 Pct Recovery = 84% Analysis Date = 04/25/14 Pct Recovery = 84% Analysis Date = 04/25/14 Pct Recovery = 84% Analysis Date = 04/14/14 Pct Recovery = 84% Analysis Date = 04/14/14 Pct Recovery = 84% Analysis Date = 04/03/14 Pct Recovery = 84% Analysis Date = 04/03/14 Pct Recovery = 84% Analysis Date = 03/23/14 Pct Recovery = 84% Analysis Date = 03/23/14 Pct Recovery = 84% Analysis Date = 03/13/14 Pct Recovery = 84% Analysis Date = 03/13/14 Pct Recovery = 84% Analysis Date = 03/02/14 Pct Recovery = 83% Analysis Date = 03/02/14 Pct Recovery = 83% Analysis Date = 02/19/14 Pct Recovery = 83% Analysis Date = 02/19/14 Pct Recovery = 83% Analysis Date = 02/08/14 Pct Recovery = 83% Analysis Date = 02/08/14 Pct Recovery = 83% Analysis Date = 01/28/14 Pct Recovery = 83% Analysis Date = 01/28/14 Pct Recovery = 83% Analysis Date = 01/18/14 Pct Recovery = 83% Analysis Date = 01/18/14 Pct Recovery = 83% Analysis Date = 01/07/14 Pct Recovery = 83% Analysis Date = 01/07/14 Pct Recovery = 83% Analysis Date = 12/27/13 Pct Recovery = 83% Analysis Date = 12/27/13 Pct Recovery = 83% Analysis Date = 12/16/13 Pct Recovery = 83% Analysis Date = 12/16/13 Pct Recovery = 83% Analysis Date = 12/06/13 Pct Recovery = 83% Analysis Date = 12/06/13 Pct Recovery = 83% Analysis Date = 11/25/13 Pct Recovery = 83% Analysis Date = 11/25/13 Pct Recovery = 83% Analysis Date = 11/14/13 Pct Recovery = 83% Analysis Date = 11/14/13 Pct Recovery = 83% Analysis Date = 11/03/13 Pct Recovery = 83% Analysis Date = 11/03/13 Pct Recovery = 83% Analysis Date = 10/23/13 Pct Recovery = 83% Analysis Date = 10/23/13 Pct Recovery = 83% Analysis Date = 10/13/13 Pct Recovery = 84% Analysis Date = 10/13/13 Pct Recovery = 84% Analysis Date = 10/02/13 Pct Recovery = 84% Analysis Date = 10/02/13 Pct Recovery = 84% Analysis Date = 09/21/13 Pct Recovery = 84% Analysis Date = 09/21/13 Pct Recovery = 84% Analysis Date = 09/10/13 Pct Recovery = 84% Analysis Date = 09/10/13 Pct Recovery = 84% Analysis Date = 08/31/13 Pct Recovery = 84% Analysis Date = 08/31/13 Pct Recovery = 84% Analysis Date = 08/20/13 Pct Recovery = 84% Analysis Date = 08/20/13 Pct Recovery = 84% Analysis Date = 08/09/13 Pct Recovery = 84% Analysis Date = 08/09/13 Pct Recovery = 84% Analysis Date = 07/29/13 Pct Recovery = 84% Analysis Date = 07/29/13 Pct Recovery = 84% Analysis Date = 07/19/13 Pct Recovery = 84% Analysis Date = 07/19/13 Pct Recovery = 84% Analysis Date = 07/08/13 Pct Recovery = 84% Analysis Date = 07/08/13 Pct Recovery = 84% Analysis Date = 06/27/13 Pct Recovery = 84% Analysis Date = 06/27/13 Pct Recovery = 84% Analysis Date = 06/16/13 Pct Recovery = 84% Analysis Date = 06/16/13 Pct Recovery = 84% Analysis Date = 06/05/13 Pct Recovery = 84% Analysis Date = 06/05/13 Pct Recovery = 84% Analysis Date = 05/26/13 Pct Recovery = 84% Analysis Date = 05/26/13 Pct Recovery = 84% Analysis Date = 05/15/13 Pct Recovery = 85% Analysis Date = 05/15/13 Pct Recovery = 85% Analysis Date = 05/04/13 Pct Recovery = 85% Analysis Date = 05/04/13 Pct Recovery = 85% Analysis Date = 04/23/13 Pct Recovery = 85% Analysis Date = 04/23/13 Pct Recovery = 85% Analysis Date = 04/13/13 Pct Recovery = 85% Analysis Date = 04/13/13 Pct Recovery = 85% Analysis Date = 04/02/13 Pct Recovery = 85% Analysis Date = 04/02/13 Pct Recovery = 85% Analysis Date = 03/22/13 Pct Recovery = 85% Analysis Date = 03/22/13 Pct Recovery = 85% Analysis Date = 03/11/13 Pct Recovery = 85% Analysis Date = 03/11/13 Pct Recovery = 85% Analysis Date = 02/28/13 Pct Recovery = 85% Analysis Date = 02/28/13 Pct Recovery = 85% Analysis Date = 02/18/13 Pct Recovery = 85% Analysis Date = 02/18/13 Pct Recovery = 85% Analysis Date = 02/07/13 Pct Recovery = 85% Analysis Date = 02/07/13 Pct Recovery = 85% Analysis Date = 01/27/13 Pct Recovery = 85% Analysis Date = 01/27/13 Pct Recovery = 85% Analysis Date = 01/16/13 Pct Recovery = 85% Analysis Date = 01/16/13 Pct Recovery = 85% Analysis Date = 01/06/13 Pct Recovery = 85% Analysis Date = 01/06/13 Pct Recovery = 85% Analysis Date = 12/26/12 Pct Recovery = 85% Analysis Date = 12/26/12 Pct Recovery = 85% Analysis Date = 12/15/12 Pct Recovery = 85% Analysis Date = 12/15/12 Pct Recovery = 85% Analysis Date = 12/04/12 Pct Recovery = 85% Analysis Date = 12/04/12 Pct Recovery = 85% Analysis Date = 11/23/12 Pct Recovery = 85% Analysis Date = 11/23/12 Pct Recovery = 85% Analysis Date = 11/13/12 Pct Recovery = 85% Analysis Date = 11/13/12 Pct Recovery = 85% Analysis Date = 11/02/12 Pct Recovery = 85% Analysis Date = 11/02/12 Pct Recovery = 85% Analysis Date = 10/22/12 Pct Recovery = 85% Analysis Date = 10/22/12 Pct Recovery = 85% Analysis Date = 10/11/12 Pct Recovery = 85% Analysis Date = 10/11/12 Pct Recovery = 85% Analysis Date = 10/01/12 Pct Recovery = 85% Analysis Date = 10/01/12 Pct Recovery = 85% Analysis Date = 09/20/12 Pct Recovery = 85% Analysis Date = 09/20/12 Pct Recovery = 85% Analysis Date = 09/09/12 Pct Recovery = 85% Analysis Date = 09/09/12 Pct Recovery = 85% Analysis Date = 08/29/12 Pct Recovery = 85% Analysis Date = 08/29/12 Pct Recovery = 85% Analysis Date = 08/18/12 Pct Recovery = 85% Analysis Date = 08/18/12 Pct Recovery = 85% Analysis Date = 08/08/12 Pct Recovery = 85% Analysis Date = 08/08/12 Pct Recovery = 85% Analysis Date = 07/28/12 Pct Recovery = 85% Analysis Date = 07/28/12 Pct Recovery = 85% Analysis Date = 07/17/12 Pct Recovery = 85% Analysis Date = 07/17/12 Pct Recovery = 85% Analysis Date = 07/06/12 Pct Recovery = 86% Analysis Date = 07/06/12 Pct Recovery = 86% Analysis Date = 06/26/12 Pct Recovery = 86% Analysis Date = 06/26/12 Pct Recovery = 86% Analysis Date = 06/15/12 Pct Recovery = 86% Analysis Date = 06/15/12 Pct Recovery = 86% Analysis Date = 06/04/12 Pct Recovery = 86% Analysis Date = 06/04/12 Pct Recovery = 86% Analysis Date = 05/24/12 Pct Recovery = 86% Analysis Date = 05/24/12 Pct Recovery = 86% Analysis Date = 05/14/12 Pct Recovery = 86% Analysis Date = 05/14/12 Pct Recovery = 86% Analysis Date = 05/03/12 Pct Recovery = 86% Analysis Date = 05/03/12 Pct Recovery = 86% Analysis Date = 04/22/12 Pct Recovery = 86% Analysis Date = 04/22/12 Pct Recovery = 86% Analysis Date = 04/11/12 Pct Recovery = 86% Analysis Date = 04/11/12 Pct Recovery = 86% Analysis Date = 03/31/12 Pct Recovery = 86% Analysis Date = 03/31/12 Pct Recovery = 86% Analysis Date = 03/21/12 Pct Recovery = 86% Analysis Date = 03/21/12 Pct Recovery = 86% Analysis Date = 03/10/12 Pct Recovery = 86% Analysis Date = 03/10/12 Pct Recovery = 86% Analysis Date = 02/28/12 Pct Recovery = 86% Analysis Date = 02/28/12 Pct Recovery = 86% Analysis Date = 02/17/12 Pct Recovery = 86% Analysis Date = 02/17/12 Pct Recovery = 86% Analysis Date = 02/07/12 Pct Recovery = 86% Analysis Date = 02/07/12 Pct Recovery = 86% Analysis Date = 01/27/12 Pct Recovery = 86% Analysis Date = 01/27/12 Pct Recovery = 86% Analysis Date = 01/16/12 Pct Recovery = 86% Analysis Date = 01/16/12 Pct Recovery = 86% Analysis Date = 01/05/12 Pct Recovery = 86% Analysis Date = 01/05/12 Pct Recovery = 86% Analysis Date = 12/25/11 Pct Recovery = 86% Analysis Date = 12/25/11 Pct Recovery = 86% Analysis Date = 12/15/11 Pct Recovery = 86% Analysis Date = 12/15/11 Pct Recovery = 86% Analysis Date = 12/04/11 Pct Recovery = 86% Analysis Date = 12/04/11 Pct Recovery = 86% Analysis Date = 11/23/11 Pct Recovery = 86% Analysis Date = 11/23/11 Pct Recovery = 86% Analysis Date = 11/12/11 Pct Recovery = 86% Analysis Date = 11/12/11 Pct Recovery = 86% Analysis Date = 11/02/11 Pct Recovery = 86% Analysis Date = 11/02/11 Pct Recovery = 86% Analysis Date = 10/22/11 Pct Recovery = 86% Analysis Date = 10/22/11 Pct Recovery = 86% Analysis Date = 10/11/11 Pct Recovery = 86% Analysis Date = 10/11/11 Pct Recovery = 86% Analysis Date = 09/30/11 Pct Recovery = 86% Analysis Date = 09/30/11 Pct Recovery = 86% Analysis Date = 09/19/11 Pct Recovery = 86% Analysis Date = 09/19/11 Pct Recovery = 86% Analysis Date = 09/09/11 Pct Recovery = 86% Analysis Date = 09/09/11 Pct Recovery = 86% Analysis Date = 08/29/11 Pct Recovery = 86% Analysis Date = 08/29/11 Pct Recovery = 86% Analysis Date = 08/18/11 Pct Recovery = 86% Analysis Date = 08/18/11 Pct Recovery = 86% Analysis Date = 08/07/11 Pct Recovery = 86% Analysis Date = 08/07/11 Pct Recovery = 86% Analysis Date = 07/28/11 Pct Recovery = 86% Analysis Date = 07/28/11 Pct Recovery = 86% Analysis Date = 07/17/11 Pct Recovery = 86% Analysis Date = 07/17/11 Pct Recovery = 86% Analysis Date = 07/06/11 Pct Recovery = 86% Analysis Date = 07/06/11 Pct Recovery = 86% Analysis Date = 06/25/11 Pct Recovery = 86% Analysis Date = 06/25/11 Pct Recovery = 86% Analysis Date = 06/14/11 Pct Recovery = 86% Analysis Date = 06/14/11 Pct Recovery = 86% Analysis Date = 06/04/11 Pct Recovery = 86% Analysis Date = 06/04/11 Pct Recovery = 86% Analysis Date = 05/24/11 Pct Recovery = 86% Analysis Date = 05/24/11 Pct Recovery = 86% Analysis Date = 05/13/11 Pct Recovery = 86% Analysis Date = 05/13/11 Pct Recovery = 86% Analysis Date = 05/02/11 Pct Recovery = 86% Analysis Date = 05/02/11 Pct Recovery = 86% Analysis Date = 04/22/11 Pct Recovery = 86% Analysis Date = 04/22/11 Pct Recovery = 86% Analysis Date = 04/11/11 Pct Recovery = 86% Analysis Date = 04/11/11 Pct Recovery = 86% Analysis Date = 03/31/11 Pct Recovery = 86% Analysis Date = 03/31/11 Pct Recovery = 86% Analysis Date = 03/20/11 Pct Recovery = 86% Analysis Date = 03/20/11 Pct Recovery = 86% Analysis Date = 03/10/11 Pct Recovery = 86% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
17-ALPHA-ESTRADIOL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 72 89% 25% 88% 13%
Total 72 89% 25% 88% 13%

Sample Statistics
17-ALPHA-ESTRADIOL

Characteristic N % % Basis
Plotted 72 91% Spiked
Estimated Values 0 0% Spiked
Deleted Values 2 2% Spiked + Not Spiked
Spiked, Censored 3 4% Spiked
Spiked 80 .  
False Negatives 4 5% 4 out of 79
Not Spiked 51 .  
False Positives 1 2% 1 out of 50

BQS OBSP Determination:
17-ALPHA-ETHYNYLESTRADIOL
METHOD: 4434 , TESTIDCODE: 64529GM005
Open Data Set

Analysis Date = 04/14/14 SpikeMix = ERA 0415-13-01.1A: 50 µl & Abs 071513: 50 µl Pct Recovery = 87% Analysis Date = 03/05/14 SpikeMix = ERA 0415-13-01.1A: 50 µl & Abs 060413: 50 µl & Abs 071513: 50 µl Pct Recovery = 71% Analysis Date = 02/25/14 SpikeMix = ERA 0415-13-01.1A: 50 µl & Abs 050813: 50 µl Pct Recovery = 61% Analysis Date = 03/14/14 SpikeMix = Supelco LB99393: 50 µl & Abs 050813: 50 µl Pct Recovery = 67% Analysis Date = 03/14/14 SpikeMix = Supelco LB99393: 50 µl & Abs 060413: 50 µl & Abs 071513: 50 µl Pct Recovery = 58% Analysis Date = 03/27/12 SpikeMix = Crescent 162776: 100 µl Pct Recovery = 96% Analysis Date = 01/27/12 SpikeMix = Supelco LB77167: 100 µl Pct Recovery = 82% Analysis Date = 10/13/11 SpikeMix = Supelco LB77167: 100 µl Pct Recovery = 74% Analysis Date = 06/07/11 SpikeMix = Supelco LB77167: 100 µl Pct Recovery = 85% Analysis Date = 03/10/11 SpikeMix = Crescent 162776: 100 µl Pct Recovery = 75% Analysis Date = 06/23/11 SpikeMix = Crescent 162776: 100 µl Pct Recovery = 82% Analysis Date = 12/15/16 SpikeMix = Abs 061416H: 50 µl & ChemService 5016100: 50 µl Pct Recovery = 84% Analysis Date = 08/19/16 SpikeMix = Supelco LC20140V: 50 µl & Spex Organics TS160420010: 50 µl Pct Recovery = 90% Analysis Date = 08/11/16 SpikeMix = ChemService 5016100: 50 µl & Spex Organics TS160420010: 50 µl Pct Recovery = 82% Analysis Date = 04/01/15 SpikeMix = ERA 0227-14-07.2: 60 µl & ChemService 2561700: 60 µl Pct Recovery = 83% Analysis Date = 04/01/15 SpikeMix = Spex Organics E1140505004: 60 µl & Supelco LC06946: 60 µl Pct Recovery = 64% Analysis Date = 02/12/15 SpikeMix = Supelco LC06946: 60 µl & Abs 042114: 60 µl Pct Recovery = 63% Analysis Date = 12/09/14 SpikeMix = Abs 031014: 60 µl & Supelco LC06946: 60 µl Pct Recovery = 67% Analysis Date = 09/23/14 SpikeMix = Supelco LC06946: 60 µl & ChemService 2561700: 60 µl Pct Recovery = 75% Analysis Date = 04/14/14 SpikeMix = ERA 0415-13-01.1A: 20 µl & ERA 0415-13-01.2A: 20 µl & Abs 060413: 20 µl Pct Recovery = 77% Analysis Date = 09/16/13 SpikeMix = ERA 0415-13-01.1A: 20 µl & ERA 0415-13-01.2A: 20 µl & Abs 060413: 20 µl Pct Recovery = 75% Analysis Date = 06/27/13 SpikeMix = ERA 0415-13-01.1A: 20 µl & Spex Organics T1130423008: 20 µl Pct Recovery = 65% Analysis Date = 01/23/14 SpikeMix = Supelco LB99393: 20 µl & ERA 0415-13-01.2A: 20 µl & Abs 060413: 20 µl Pct Recovery = 66% Analysis Date = 12/09/13 SpikeMix = Supelco LB99393: 20 µl & Spex Organics T1130423008: 20 µl Pct Recovery = 66% Analysis Date = 07/19/13 SpikeMix = Supelco LB99393: 20 µl & ERA 0415-13-01.2A: 20 µl Pct Recovery = 71% Analysis Date = 06/04/13 SpikeMix = Supelco LB99393: 20 µl & Spex Organics T1130423008: 20 µl Pct Recovery = 63% Analysis Date = 01/08/16 SpikeMix = Spex Organics EN150501025: 60 µl & ERA 0601-15-04: 60 µl Pct Recovery = 80% Analysis Date = 04/22/13 SpikeMix = ERA 0507-12-04.1: 50 µl & Restek A089631: 50 µl Pct Recovery = 84% Analysis Date = 12/18/12 SpikeMix = ERA 0507-12-04.1: 50 µl & Restek A089631: 50 µl Pct Recovery = 80% Analysis Date = 11/07/12 SpikeMix = ERA 0507-12-04.1: 50 µl & ERA 0511-12-02: 50 µl Pct Recovery = 67% Analysis Date = 04/03/13 SpikeMix = Spex Organics T1120525010: 50 µl & Restek A089631: 50 µl Pct Recovery = 78% Analysis Date = 12/18/12 SpikeMix = Spex Organics T1120525010: 50 µl & Supelco LB92781: 50 µl Pct Recovery = 72% Analysis Date = 07/12/16 SpikeMix = Spex Organics EN150501025: 50 µl & ERA 0601-15-04: 50 µl Pct Recovery = 85% Analysis Date = 06/24/16 SpikeMix = ERA 0601-15-04: 50 µl & ChemService 4073900: 50 µl Pct Recovery = 52% Analysis Date = 03/07/16 SpikeMix = Abs 041515: 50 µl & ERA 0601-15-04: 50 µl Pct Recovery = 102% Analysis Date = 12/10/15 SpikeMix = Abs 041515: 50 µl & ERA 0601-15-04: 50 µl Pct Recovery = 82% Analysis Date = 09/14/15 SpikeMix = ERA 0601-15-04: 50 µl & ChemService 4073900: 50 µl Pct Recovery = 98% Analysis Date = 08/10/15 SpikeMix = ERA 0601-15-04: 50 µl & Crescent 04EE007: 50 µl Pct Recovery = 86% Analysis Date = 02/01/17 SpikeMix = Supelco LC20140V: 30 µl & Abs 052616: 30 µl Pct Recovery = 86% Analysis Date = 12/29/16 SpikeMix = ChemService 5016100: 30 µl & Abs 052616: 30 µl Pct Recovery = 77% Analysis Date = 09/21/16 SpikeMix = ChemService 5016200: 30 µl & ChemService 5016100: 30 µl Pct Recovery = 141% Analysis Date = 11/05/14 SpikeMix = ERA 0227-14-07.2: 30 µl & Abs 042114: 30 µl Pct Recovery = 87% Analysis Date = 09/04/14 SpikeMix = ERA 0227-14-07.2: 30 µl & Spex Organics E1140505004: 30 µl Pct Recovery = 85% Analysis Date = 07/28/14 SpikeMix = ERA 0227-14-07.2: 30 µl & ChemService 2561700: 30 µl Pct Recovery = 109% Analysis Date = 07/14/14 SpikeMix = ERA 0227-14-07.2: 30 µl & Abs 031014: 30 µl Pct Recovery = 100% Analysis Date = 01/29/15 SpikeMix = Abs 031014: 30 µl & Supelco LC06946: 30 µl Pct Recovery = 72% Analysis Date = 12/23/14 SpikeMix = Spex Organics E1140505004: 30 µl & Supelco LC06946: 30 µl Pct Recovery = 72% Analysis Date = 12/16/14 SpikeMix = Supelco LC06946: 30 µl & Abs 042114: 30 µl Pct Recovery = 67% Analysis Date = 07/27/12 SpikeMix = Supelco LB77167: 25 µl Pct Recovery = 68% Analysis Date = 04/17/12 SpikeMix = Supelco LB77167: 25 µl Pct Recovery = 91% Analysis Date = 04/06/12 SpikeMix = Crescent 162776: 25 µl Pct Recovery = 103% Analysis Date = 04/04/12 SpikeMix = Supelco LB77167: 25 µl Pct Recovery = 93% Analysis Date = 11/17/11 SpikeMix = Crescent 162776: 25 µl Pct Recovery = 80% Analysis Date = 10/12/11 SpikeMix = Crescent 162776: 25 µl Pct Recovery = 69% Analysis Date = 09/29/11 SpikeMix = Supelco LB77167: 25 µl Pct Recovery = 75% Analysis Date = 07/25/11 SpikeMix = Crescent 162776: 25 µl Pct Recovery = 59% Analysis Date = 05/19/11 SpikeMix = Supelco LB77167: 25 µl Pct Recovery = 86% Analysis Date = 03/31/11 SpikeMix = Supelco LB77167: 25 µl Pct Recovery = 93% Analysis Date = 05/09/11 SpikeMix = Crescent 162776: 25 µl Pct Recovery = 73% Analysis Date = 01/08/16 SpikeMix = ERA 0601-15-04: 30 µl & Crescent 04EE007: 30 µl Pct Recovery = 98% Analysis Date = 11/01/12 SpikeMix = ERA 0507-12-04.1: 25 µl & Abs 051512: 25 µl Pct Recovery = 83% Analysis Date = 04/03/13 SpikeMix = Spex Organics T1120525010: 25 µl & Abs 051512: 25 µl Pct Recovery = 66% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120525010: 25 µl & ERA 0511-12-02: 25 µl Pct Recovery = 135% Analysis Date = 08/29/12 SpikeMix = Spex Organics T1120525010: 25 µl Pct Recovery = 92% Analysis Date = 02/01/17 Pct Recovery = 91% Analysis Date = 01/21/17 Pct Recovery = 91% Analysis Date = 01/21/17 Pct Recovery = 91% Analysis Date = 01/10/17 Pct Recovery = 91% Analysis Date = 01/10/17 Pct Recovery = 91% Analysis Date = 12/30/16 Pct Recovery = 91% Analysis Date = 12/30/16 Pct Recovery = 91% Analysis Date = 12/19/16 Pct Recovery = 90% Analysis Date = 12/19/16 Pct Recovery = 90% Analysis Date = 12/09/16 Pct Recovery = 90% Analysis Date = 12/09/16 Pct Recovery = 90% Analysis Date = 11/28/16 Pct Recovery = 90% Analysis Date = 11/28/16 Pct Recovery = 90% Analysis Date = 11/17/16 Pct Recovery = 90% Analysis Date = 11/17/16 Pct Recovery = 90% Analysis Date = 11/06/16 Pct Recovery = 90% Analysis Date = 11/06/16 Pct Recovery = 90% Analysis Date = 10/27/16 Pct Recovery = 90% Analysis Date = 10/27/16 Pct Recovery = 90% Analysis Date = 10/16/16 Pct Recovery = 89% Analysis Date = 10/16/16 Pct Recovery = 89% Analysis Date = 10/05/16 Pct Recovery = 89% Analysis Date = 10/05/16 Pct Recovery = 89% Analysis Date = 09/24/16 Pct Recovery = 89% Analysis Date = 09/24/16 Pct Recovery = 89% Analysis Date = 09/13/16 Pct Recovery = 89% Analysis Date = 09/13/16 Pct Recovery = 89% Analysis Date = 09/03/16 Pct Recovery = 89% Analysis Date = 09/03/16 Pct Recovery = 89% Analysis Date = 08/23/16 Pct Recovery = 89% Analysis Date = 08/23/16 Pct Recovery = 89% Analysis Date = 08/12/16 Pct Recovery = 88% Analysis Date = 08/12/16 Pct Recovery = 88% Analysis Date = 08/01/16 Pct Recovery = 88% Analysis Date = 08/01/16 Pct Recovery = 88% Analysis Date = 07/22/16 Pct Recovery = 88% Analysis Date = 07/22/16 Pct Recovery = 88% Analysis Date = 07/11/16 Pct Recovery = 88% Analysis Date = 07/11/16 Pct Recovery = 88% Analysis Date = 06/30/16 Pct Recovery = 88% Analysis Date = 06/30/16 Pct Recovery = 88% Analysis Date = 06/19/16 Pct Recovery = 88% Analysis Date = 06/19/16 Pct Recovery = 88% Analysis Date = 06/08/16 Pct Recovery = 87% Analysis Date = 06/08/16 Pct Recovery = 87% Analysis Date = 05/29/16 Pct Recovery = 87% Analysis Date = 05/29/16 Pct Recovery = 87% Analysis Date = 05/18/16 Pct Recovery = 87% Analysis Date = 05/18/16 Pct Recovery = 87% Analysis Date = 05/07/16 Pct Recovery = 87% Analysis Date = 05/07/16 Pct Recovery = 87% Analysis Date = 04/26/16 Pct Recovery = 87% Analysis Date = 04/26/16 Pct Recovery = 87% Analysis Date = 04/16/16 Pct Recovery = 86% Analysis Date = 04/16/16 Pct Recovery = 86% Analysis Date = 04/05/16 Pct Recovery = 86% Analysis Date = 04/05/16 Pct Recovery = 86% Analysis Date = 03/25/16 Pct Recovery = 86% Analysis Date = 03/25/16 Pct Recovery = 86% Analysis Date = 03/14/16 Pct Recovery = 86% Analysis Date = 03/14/16 Pct Recovery = 86% Analysis Date = 03/03/16 Pct Recovery = 86% Analysis Date = 03/03/16 Pct Recovery = 86% Analysis Date = 02/22/16 Pct Recovery = 86% Analysis Date = 02/22/16 Pct Recovery = 86% Analysis Date = 02/11/16 Pct Recovery = 85% Analysis Date = 02/11/16 Pct Recovery = 85% Analysis Date = 01/31/16 Pct Recovery = 85% Analysis Date = 01/31/16 Pct Recovery = 85% Analysis Date = 01/20/16 Pct Recovery = 85% Analysis Date = 01/20/16 Pct Recovery = 85% Analysis Date = 01/10/16 Pct Recovery = 85% Analysis Date = 01/10/16 Pct Recovery = 85% Analysis Date = 12/30/15 Pct Recovery = 85% Analysis Date = 12/30/15 Pct Recovery = 85% Analysis Date = 12/19/15 Pct Recovery = 85% Analysis Date = 12/19/15 Pct Recovery = 85% Analysis Date = 12/08/15 Pct Recovery = 84% Analysis Date = 12/08/15 Pct Recovery = 84% Analysis Date = 11/28/15 Pct Recovery = 84% Analysis Date = 11/28/15 Pct Recovery = 84% Analysis Date = 11/17/15 Pct Recovery = 84% Analysis Date = 11/17/15 Pct Recovery = 84% Analysis Date = 11/06/15 Pct Recovery = 84% Analysis Date = 11/06/15 Pct Recovery = 84% Analysis Date = 10/26/15 Pct Recovery = 84% Analysis Date = 10/26/15 Pct Recovery = 84% Analysis Date = 10/15/15 Pct Recovery = 84% Analysis Date = 10/15/15 Pct Recovery = 84% Analysis Date = 10/05/15 Pct Recovery = 83% Analysis Date = 10/05/15 Pct Recovery = 83% Analysis Date = 09/24/15 Pct Recovery = 83% Analysis Date = 09/24/15 Pct Recovery = 83% Analysis Date = 09/13/15 Pct Recovery = 83% Analysis Date = 09/13/15 Pct Recovery = 83% Analysis Date = 09/02/15 Pct Recovery = 83% Analysis Date = 09/02/15 Pct Recovery = 83% Analysis Date = 08/23/15 Pct Recovery = 83% Analysis Date = 08/23/15 Pct Recovery = 83% Analysis Date = 08/12/15 Pct Recovery = 83% Analysis Date = 08/12/15 Pct Recovery = 83% Analysis Date = 08/01/15 Pct Recovery = 82% Analysis Date = 08/01/15 Pct Recovery = 82% Analysis Date = 07/21/15 Pct Recovery = 82% Analysis Date = 07/21/15 Pct Recovery = 82% Analysis Date = 07/10/15 Pct Recovery = 82% Analysis Date = 07/10/15 Pct Recovery = 82% Analysis Date = 06/30/15 Pct Recovery = 82% Analysis Date = 06/30/15 Pct Recovery = 82% Analysis Date = 06/19/15 Pct Recovery = 82% Analysis Date = 06/19/15 Pct Recovery = 82% Analysis Date = 06/08/15 Pct Recovery = 82% Analysis Date = 06/08/15 Pct Recovery = 82% Analysis Date = 05/28/15 Pct Recovery = 81% Analysis Date = 05/28/15 Pct Recovery = 81% Analysis Date = 05/18/15 Pct Recovery = 81% Analysis Date = 05/18/15 Pct Recovery = 81% Analysis Date = 05/07/15 Pct Recovery = 81% Analysis Date = 05/07/15 Pct Recovery = 81% Analysis Date = 04/26/15 Pct Recovery = 81% Analysis Date = 04/26/15 Pct Recovery = 81% Analysis Date = 04/15/15 Pct Recovery = 81% Analysis Date = 04/15/15 Pct Recovery = 81% Analysis Date = 04/04/15 Pct Recovery = 80% Analysis Date = 04/04/15 Pct Recovery = 80% Analysis Date = 03/25/15 Pct Recovery = 80% Analysis Date = 03/25/15 Pct Recovery = 80% Analysis Date = 03/14/15 Pct Recovery = 80% Analysis Date = 03/14/15 Pct Recovery = 80% Analysis Date = 03/03/15 Pct Recovery = 80% Analysis Date = 03/03/15 Pct Recovery = 80% Analysis Date = 02/20/15 Pct Recovery = 80% Analysis Date = 02/20/15 Pct Recovery = 80% Analysis Date = 02/10/15 Pct Recovery = 80% Analysis Date = 02/10/15 Pct Recovery = 80% Analysis Date = 01/30/15 Pct Recovery = 79% Analysis Date = 01/30/15 Pct Recovery = 79% Analysis Date = 01/19/15 Pct Recovery = 79% Analysis Date = 01/19/15 Pct Recovery = 79% Analysis Date = 01/08/15 Pct Recovery = 79% Analysis Date = 01/08/15 Pct Recovery = 79% Analysis Date = 12/28/14 Pct Recovery = 79% Analysis Date = 12/28/14 Pct Recovery = 79% Analysis Date = 12/18/14 Pct Recovery = 79% Analysis Date = 12/18/14 Pct Recovery = 79% Analysis Date = 12/07/14 Pct Recovery = 78% Analysis Date = 12/07/14 Pct Recovery = 78% Analysis Date = 11/26/14 Pct Recovery = 78% Analysis Date = 11/26/14 Pct Recovery = 78% Analysis Date = 11/15/14 Pct Recovery = 78% Analysis Date = 11/15/14 Pct Recovery = 78% Analysis Date = 11/05/14 Pct Recovery = 78% Analysis Date = 11/05/14 Pct Recovery = 78% Analysis Date = 10/25/14 Pct Recovery = 77% Analysis Date = 10/25/14 Pct Recovery = 77% Analysis Date = 10/14/14 Pct Recovery = 77% Analysis Date = 10/14/14 Pct Recovery = 77% Analysis Date = 10/03/14 Pct Recovery = 77% Analysis Date = 10/03/14 Pct Recovery = 77% Analysis Date = 09/23/14 Pct Recovery = 77% Analysis Date = 09/23/14 Pct Recovery = 77% Analysis Date = 09/12/14 Pct Recovery = 77% Analysis Date = 09/12/14 Pct Recovery = 77% Analysis Date = 09/01/14 Pct Recovery = 76% Analysis Date = 09/01/14 Pct Recovery = 76% Analysis Date = 08/21/14 Pct Recovery = 76% Analysis Date = 08/21/14 Pct Recovery = 76% Analysis Date = 08/10/14 Pct Recovery = 76% Analysis Date = 08/10/14 Pct Recovery = 76% Analysis Date = 07/31/14 Pct Recovery = 76% Analysis Date = 07/31/14 Pct Recovery = 76% Analysis Date = 07/20/14 Pct Recovery = 76% Analysis Date = 07/20/14 Pct Recovery = 76% Analysis Date = 07/09/14 Pct Recovery = 76% Analysis Date = 07/09/14 Pct Recovery = 76% Analysis Date = 06/28/14 Pct Recovery = 76% Analysis Date = 06/28/14 Pct Recovery = 76% Analysis Date = 06/18/14 Pct Recovery = 76% Analysis Date = 06/18/14 Pct Recovery = 76% Analysis Date = 06/07/14 Pct Recovery = 76% Analysis Date = 06/07/14 Pct Recovery = 76% Analysis Date = 05/27/14 Pct Recovery = 76% Analysis Date = 05/27/14 Pct Recovery = 76% Analysis Date = 05/16/14 Pct Recovery = 76% Analysis Date = 05/16/14 Pct Recovery = 76% Analysis Date = 05/05/14 Pct Recovery = 76% Analysis Date = 05/05/14 Pct Recovery = 76% Analysis Date = 04/25/14 Pct Recovery = 76% Analysis Date = 04/25/14 Pct Recovery = 76% Analysis Date = 04/14/14 Pct Recovery = 76% Analysis Date = 04/14/14 Pct Recovery = 76% Analysis Date = 04/03/14 Pct Recovery = 76% Analysis Date = 04/03/14 Pct Recovery = 76% Analysis Date = 03/23/14 Pct Recovery = 76% Analysis Date = 03/23/14 Pct Recovery = 76% Analysis Date = 03/13/14 Pct Recovery = 76% Analysis Date = 03/13/14 Pct Recovery = 76% Analysis Date = 03/02/14 Pct Recovery = 76% Analysis Date = 03/02/14 Pct Recovery = 76% Analysis Date = 02/19/14 Pct Recovery = 76% Analysis Date = 02/19/14 Pct Recovery = 76% Analysis Date = 02/08/14 Pct Recovery = 76% Analysis Date = 02/08/14 Pct Recovery = 76% Analysis Date = 01/28/14 Pct Recovery = 76% Analysis Date = 01/28/14 Pct Recovery = 76% Analysis Date = 01/18/14 Pct Recovery = 76% Analysis Date = 01/18/14 Pct Recovery = 76% Analysis Date = 01/07/14 Pct Recovery = 76% Analysis Date = 01/07/14 Pct Recovery = 76% Analysis Date = 12/27/13 Pct Recovery = 76% Analysis Date = 12/27/13 Pct Recovery = 76% Analysis Date = 12/16/13 Pct Recovery = 76% Analysis Date = 12/16/13 Pct Recovery = 76% Analysis Date = 12/06/13 Pct Recovery = 76% Analysis Date = 12/06/13 Pct Recovery = 76% Analysis Date = 11/25/13 Pct Recovery = 76% Analysis Date = 11/25/13 Pct Recovery = 76% Analysis Date = 11/14/13 Pct Recovery = 76% Analysis Date = 11/14/13 Pct Recovery = 76% Analysis Date = 11/03/13 Pct Recovery = 77% Analysis Date = 11/03/13 Pct Recovery = 77% Analysis Date = 10/23/13 Pct Recovery = 77% Analysis Date = 10/23/13 Pct Recovery = 77% Analysis Date = 10/13/13 Pct Recovery = 77% Analysis Date = 10/13/13 Pct Recovery = 77% Analysis Date = 10/02/13 Pct Recovery = 77% Analysis Date = 10/02/13 Pct Recovery = 77% Analysis Date = 09/21/13 Pct Recovery = 77% Analysis Date = 09/21/13 Pct Recovery = 77% Analysis Date = 09/10/13 Pct Recovery = 77% Analysis Date = 09/10/13 Pct Recovery = 77% Analysis Date = 08/31/13 Pct Recovery = 77% Analysis Date = 08/31/13 Pct Recovery = 77% Analysis Date = 08/20/13 Pct Recovery = 77% Analysis Date = 08/20/13 Pct Recovery = 77% Analysis Date = 08/09/13 Pct Recovery = 77% Analysis Date = 08/09/13 Pct Recovery = 77% Analysis Date = 07/29/13 Pct Recovery = 77% Analysis Date = 07/29/13 Pct Recovery = 77% Analysis Date = 07/19/13 Pct Recovery = 77% Analysis Date = 07/19/13 Pct Recovery = 77% Analysis Date = 07/08/13 Pct Recovery = 77% Analysis Date = 07/08/13 Pct Recovery = 77% Analysis Date = 06/27/13 Pct Recovery = 77% Analysis Date = 06/27/13 Pct Recovery = 77% Analysis Date = 06/16/13 Pct Recovery = 77% Analysis Date = 06/16/13 Pct Recovery = 77% Analysis Date = 06/05/13 Pct Recovery = 78% Analysis Date = 06/05/13 Pct Recovery = 78% Analysis Date = 05/26/13 Pct Recovery = 78% Analysis Date = 05/26/13 Pct Recovery = 78% Analysis Date = 05/15/13 Pct Recovery = 78% Analysis Date = 05/15/13 Pct Recovery = 78% Analysis Date = 05/04/13 Pct Recovery = 78% Analysis Date = 05/04/13 Pct Recovery = 78% Analysis Date = 04/23/13 Pct Recovery = 78% Analysis Date = 04/23/13 Pct Recovery = 78% Analysis Date = 04/13/13 Pct Recovery = 78% Analysis Date = 04/13/13 Pct Recovery = 78% Analysis Date = 04/02/13 Pct Recovery = 79% Analysis Date = 04/02/13 Pct Recovery = 79% Analysis Date = 03/22/13 Pct Recovery = 79% Analysis Date = 03/22/13 Pct Recovery = 79% Analysis Date = 03/11/13 Pct Recovery = 79% Analysis Date = 03/11/13 Pct Recovery = 79% Analysis Date = 02/28/13 Pct Recovery = 79% Analysis Date = 02/28/13 Pct Recovery = 79% Analysis Date = 02/18/13 Pct Recovery = 79% Analysis Date = 02/18/13 Pct Recovery = 79% Analysis Date = 02/07/13 Pct Recovery = 79% Analysis Date = 02/07/13 Pct Recovery = 79% Analysis Date = 01/27/13 Pct Recovery = 80% Analysis Date = 01/27/13 Pct Recovery = 80% Analysis Date = 01/16/13 Pct Recovery = 80% Analysis Date = 01/16/13 Pct Recovery = 80% Analysis Date = 01/06/13 Pct Recovery = 80% Analysis Date = 01/06/13 Pct Recovery = 80% Analysis Date = 12/26/12 Pct Recovery = 80% Analysis Date = 12/26/12 Pct Recovery = 80% Analysis Date = 12/15/12 Pct Recovery = 80% Analysis Date = 12/15/12 Pct Recovery = 80% Analysis Date = 12/04/12 Pct Recovery = 80% Analysis Date = 12/04/12 Pct Recovery = 80% Analysis Date = 11/23/12 Pct Recovery = 81% Analysis Date = 11/23/12 Pct Recovery = 81% Analysis Date = 11/13/12 Pct Recovery = 81% Analysis Date = 11/13/12 Pct Recovery = 81% Analysis Date = 11/02/12 Pct Recovery = 81% Analysis Date = 11/02/12 Pct Recovery = 81% Analysis Date = 10/22/12 Pct Recovery = 81% Analysis Date = 10/22/12 Pct Recovery = 81% Analysis Date = 10/11/12 Pct Recovery = 81% Analysis Date = 10/11/12 Pct Recovery = 81% Analysis Date = 10/01/12 Pct Recovery = 81% Analysis Date = 10/01/12 Pct Recovery = 81% Analysis Date = 09/20/12 Pct Recovery = 81% Analysis Date = 09/20/12 Pct Recovery = 81% Analysis Date = 09/09/12 Pct Recovery = 81% Analysis Date = 09/09/12 Pct Recovery = 81% Analysis Date = 08/29/12 Pct Recovery = 81% Analysis Date = 08/29/12 Pct Recovery = 81% Analysis Date = 08/18/12 Pct Recovery = 81% Analysis Date = 08/18/12 Pct Recovery = 81% Analysis Date = 08/08/12 Pct Recovery = 81% Analysis Date = 08/08/12 Pct Recovery = 81% Analysis Date = 07/28/12 Pct Recovery = 81% Analysis Date = 07/28/12 Pct Recovery = 81% Analysis Date = 07/17/12 Pct Recovery = 81% Analysis Date = 07/17/12 Pct Recovery = 81% Analysis Date = 07/06/12 Pct Recovery = 81% Analysis Date = 07/06/12 Pct Recovery = 81% Analysis Date = 06/26/12 Pct Recovery = 81% Analysis Date = 06/26/12 Pct Recovery = 81% Analysis Date = 06/15/12 Pct Recovery = 81% Analysis Date = 06/15/12 Pct Recovery = 81% Analysis Date = 06/04/12 Pct Recovery = 81% Analysis Date = 06/04/12 Pct Recovery = 81% Analysis Date = 05/24/12 Pct Recovery = 81% Analysis Date = 05/24/12 Pct Recovery = 81% Analysis Date = 05/14/12 Pct Recovery = 81% Analysis Date = 05/14/12 Pct Recovery = 81% Analysis Date = 05/03/12 Pct Recovery = 81% Analysis Date = 05/03/12 Pct Recovery = 81% Analysis Date = 04/22/12 Pct Recovery = 81% Analysis Date = 04/22/12 Pct Recovery = 81% Analysis Date = 04/11/12 Pct Recovery = 81% Analysis Date = 04/11/12 Pct Recovery = 81% Analysis Date = 03/31/12 Pct Recovery = 81% Analysis Date = 03/31/12 Pct Recovery = 81% Analysis Date = 03/21/12 Pct Recovery = 81% Analysis Date = 03/21/12 Pct Recovery = 81% Analysis Date = 03/10/12 Pct Recovery = 81% Analysis Date = 03/10/12 Pct Recovery = 81% Analysis Date = 02/28/12 Pct Recovery = 81% Analysis Date = 02/28/12 Pct Recovery = 81% Analysis Date = 02/17/12 Pct Recovery = 81% Analysis Date = 02/17/12 Pct Recovery = 81% Analysis Date = 02/07/12 Pct Recovery = 81% Analysis Date = 02/07/12 Pct Recovery = 81% Analysis Date = 01/27/12 Pct Recovery = 81% Analysis Date = 01/27/12 Pct Recovery = 81% Analysis Date = 01/16/12 Pct Recovery = 81% Analysis Date = 01/16/12 Pct Recovery = 81% Analysis Date = 01/05/12 Pct Recovery = 81% Analysis Date = 01/05/12 Pct Recovery = 81% Analysis Date = 12/25/11 Pct Recovery = 81% Analysis Date = 12/25/11 Pct Recovery = 81% Analysis Date = 12/15/11 Pct Recovery = 81% Analysis Date = 12/15/11 Pct Recovery = 81% Analysis Date = 12/04/11 Pct Recovery = 81% Analysis Date = 12/04/11 Pct Recovery = 81% Analysis Date = 11/23/11 Pct Recovery = 81% Analysis Date = 11/23/11 Pct Recovery = 81% Analysis Date = 11/12/11 Pct Recovery = 81% Analysis Date = 11/12/11 Pct Recovery = 81% Analysis Date = 11/02/11 Pct Recovery = 81% Analysis Date = 11/02/11 Pct Recovery = 81% Analysis Date = 10/22/11 Pct Recovery = 81% Analysis Date = 10/22/11 Pct Recovery = 81% Analysis Date = 10/11/11 Pct Recovery = 81% Analysis Date = 10/11/11 Pct Recovery = 81% Analysis Date = 09/30/11 Pct Recovery = 81% Analysis Date = 09/30/11 Pct Recovery = 81% Analysis Date = 09/19/11 Pct Recovery = 81% Analysis Date = 09/19/11 Pct Recovery = 81% Analysis Date = 09/09/11 Pct Recovery = 81% Analysis Date = 09/09/11 Pct Recovery = 81% Analysis Date = 08/29/11 Pct Recovery = 81% Analysis Date = 08/29/11 Pct Recovery = 81% Analysis Date = 08/18/11 Pct Recovery = 81% Analysis Date = 08/18/11 Pct Recovery = 81% Analysis Date = 08/07/11 Pct Recovery = 81% Analysis Date = 08/07/11 Pct Recovery = 81% Analysis Date = 07/28/11 Pct Recovery = 81% Analysis Date = 07/28/11 Pct Recovery = 81% Analysis Date = 07/17/11 Pct Recovery = 81% Analysis Date = 07/17/11 Pct Recovery = 81% Analysis Date = 07/06/11 Pct Recovery = 81% Analysis Date = 07/06/11 Pct Recovery = 81% Analysis Date = 06/25/11 Pct Recovery = 81% Analysis Date = 06/25/11 Pct Recovery = 81% Analysis Date = 06/14/11 Pct Recovery = 81% Analysis Date = 06/14/11 Pct Recovery = 81% Analysis Date = 06/04/11 Pct Recovery = 80% Analysis Date = 06/04/11 Pct Recovery = 80% Analysis Date = 05/24/11 Pct Recovery = 80% Analysis Date = 05/24/11 Pct Recovery = 80% Analysis Date = 05/13/11 Pct Recovery = 80% Analysis Date = 05/13/11 Pct Recovery = 80% Analysis Date = 05/02/11 Pct Recovery = 80% Analysis Date = 05/02/11 Pct Recovery = 80% Analysis Date = 04/22/11 Pct Recovery = 80% Analysis Date = 04/22/11 Pct Recovery = 80% Analysis Date = 04/11/11 Pct Recovery = 80% Analysis Date = 04/11/11 Pct Recovery = 80% Analysis Date = 03/31/11 Pct Recovery = 80% Analysis Date = 03/31/11 Pct Recovery = 80% Analysis Date = 03/20/11 Pct Recovery = 80% Analysis Date = 03/20/11 Pct Recovery = 80% Analysis Date = 03/10/11 Pct Recovery = 80% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
17-ALPHA-ETHYNYLESTRADIOL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 64 81% 16% 80% 13%
Total 64 81% 16% 80% 13%

Sample Statistics
17-ALPHA-ETHYNYLESTRADIOL

Characteristic N % % Basis
Plotted 64 80% Spiked
Estimated Values 1 1% Spiked
Deleted Values 2 2% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 81 .  
False Negatives 16 20% 16 out of 80
Not Spiked 50 .  
False Positives 2 4% 2 out of 49

BQS OBSP Determination:
17-BETA-ESTRADIOL
METHOD: 4434 , TESTIDCODE: 64530GM005
Open Data Set

Analysis Date = 08/31/16 SpikeMix = Spex Organics TS160420010: 50 µl & ChemService 5016200: 50 µl Pct Recovery = 75% Analysis Date = 08/19/16 SpikeMix = Supelco LC20140V: 50 µl & Spex Organics TS160420010: 50 µl Pct Recovery = 77% Analysis Date = 08/11/16 SpikeMix = ChemService 5016100: 50 µl & Spex Organics TS160420010: 50 µl Pct Recovery = 55% Analysis Date = 01/27/12 SpikeMix = Supelco LB77167: 100 µl Pct Recovery = 76% Analysis Date = 10/13/11 SpikeMix = Supelco LB77167: 100 µl Pct Recovery = 88% Analysis Date = 03/27/12 SpikeMix = Crescent 162776: 100 µl Pct Recovery = 102% Analysis Date = 06/07/11 SpikeMix = Supelco LB77167: 100 µl Pct Recovery = 95% Analysis Date = 03/10/11 SpikeMix = Crescent 162776: 100 µl Pct Recovery = 82% Analysis Date = 06/23/11 SpikeMix = Crescent 162776: 100 µl Pct Recovery = 89% Analysis Date = 04/22/13 SpikeMix = ERA 0507-12-04.1: 50 µl & Restek A089631: 50 µl Pct Recovery = 81% Analysis Date = 12/18/12 SpikeMix = ERA 0507-12-04.1: 50 µl & Restek A089631: 50 µl Pct Recovery = 81% Analysis Date = 11/07/12 SpikeMix = ERA 0507-12-04.1: 50 µl & ERA 0511-12-02: 50 µl Pct Recovery = 87% Analysis Date = 04/03/13 SpikeMix = Spex Organics T1120525010: 50 µl & Restek A089631: 50 µl Pct Recovery = 82% Analysis Date = 12/18/12 SpikeMix = Spex Organics T1120525010: 50 µl & Supelco LB92781: 50 µl Pct Recovery = 85% Analysis Date = 04/14/14 SpikeMix = ERA 0415-13-01.1A: 50 µl & Abs 071513: 50 µl Pct Recovery = 87% Analysis Date = 03/05/14 SpikeMix = ERA 0415-13-01.1A: 50 µl & Abs 060413: 50 µl & Abs 071513: 50 µl Pct Recovery = 82% Analysis Date = 02/25/14 SpikeMix = ERA 0415-13-01.1A: 50 µl & Abs 050813: 50 µl Pct Recovery = 72% Analysis Date = 03/14/14 SpikeMix = Supelco LB99393: 50 µl & Abs 050813: 50 µl Pct Recovery = 78% Analysis Date = 03/14/14 SpikeMix = Supelco LB99393: 50 µl & Abs 060413: 50 µl & Abs 071513: 50 µl Pct Recovery = 60% Analysis Date = 02/08/13 SpikeMix = ERA 0507-12-04.1: 25 µl & Supelco LB92781: 25 µl Pct Recovery = 81% Analysis Date = 11/01/12 SpikeMix = ERA 0507-12-04.1: 25 µl & Abs 051512: 25 µl Pct Recovery = 77% Analysis Date = 04/03/13 SpikeMix = Spex Organics T1120525010: 25 µl & Abs 051512: 25 µl Pct Recovery = 68% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120525010: 25 µl & ERA 0511-12-02: 25 µl Pct Recovery = 91% Analysis Date = 08/29/12 SpikeMix = Spex Organics T1120525010: 25 µl Pct Recovery = 93% Analysis Date = 01/21/15 SpikeMix = ChemService 2561700: 60 µl & Spex Organics E1140505004: 60 µl Pct Recovery = 104% Analysis Date = 09/23/14 SpikeMix = Supelco LC06946: 60 µl & ChemService 2561700: 60 µl Pct Recovery = 114% Analysis Date = 05/06/14 SpikeMix = Abs 031014: 60 µl & ChemService 2561700: 60 µl Pct Recovery = 160% Analysis Date = 04/13/15 SpikeMix = Abs 042114: 60 µl & Spex Organics E1140505004: 60 µl Pct Recovery = 91% Analysis Date = 02/12/15 SpikeMix = Supelco LC06946: 60 µl & Abs 042114: 60 µl Pct Recovery = 79% Analysis Date = 08/26/14 SpikeMix = Abs 031014: 60 µl & Abs 042114: 60 µl Pct Recovery = 89% Analysis Date = 07/27/12 SpikeMix = Supelco LB77167: 25 µl Pct Recovery = 79% Analysis Date = 04/17/12 SpikeMix = Supelco LB77167: 25 µl Pct Recovery = 98% Analysis Date = 04/04/12 SpikeMix = Supelco LB77167: 25 µl Pct Recovery = 93% Analysis Date = 09/29/11 SpikeMix = Supelco LB77167: 25 µl Pct Recovery = 70% Analysis Date = 04/06/12 SpikeMix = Crescent 162776: 25 µl Pct Recovery = 100% Analysis Date = 11/17/11 SpikeMix = Crescent 162776: 25 µl Pct Recovery = 84% Analysis Date = 10/12/11 SpikeMix = Crescent 162776: 25 µl Pct Recovery = 90% Analysis Date = 07/25/11 SpikeMix = Crescent 162776: 25 µl Pct Recovery = 60% Analysis Date = 05/19/11 SpikeMix = Supelco LB77167: 25 µl Pct Recovery = 81% Analysis Date = 03/31/11 SpikeMix = Supelco LB77167: 25 µl Pct Recovery = 73% Analysis Date = 05/09/11 SpikeMix = Crescent 162776: 25 µl Pct Recovery = 89% Analysis Date = 04/14/14 SpikeMix = ERA 0415-13-01.1A: 20 µl & ERA 0415-13-01.2A: 20 µl & Abs 060413: 20 µl Pct Recovery = 77% Analysis Date = 09/16/13 SpikeMix = ERA 0415-13-01.1A: 20 µl & ERA 0415-13-01.2A: 20 µl & Abs 060413: 20 µl Pct Recovery = 75% Analysis Date = 06/27/13 SpikeMix = ERA 0415-13-01.1A: 20 µl & Spex Organics T1130423008: 20 µl Pct Recovery = 49% Analysis Date = 01/23/14 SpikeMix = Supelco LB99393: 20 µl & ERA 0415-13-01.2A: 20 µl & Abs 060413: 20 µl Pct Recovery = 70% Analysis Date = 12/09/13 SpikeMix = Supelco LB99393: 20 µl & Spex Organics T1130423008: 20 µl Pct Recovery = 66% Analysis Date = 07/19/13 SpikeMix = Supelco LB99393: 20 µl & ERA 0415-13-01.2A: 20 µl Pct Recovery = 76% Analysis Date = 06/04/13 SpikeMix = Supelco LB99393: 20 µl & Spex Organics T1130423008: 20 µl Pct Recovery = 73% Analysis Date = 01/07/16 SpikeMix = Crescent 04EE007: 60 µl & Abs 041515: 60 µl Pct Recovery = 81% Analysis Date = 01/08/16 SpikeMix = Spex Organics EN150501025: 60 µl & ERA 0601-15-04: 60 µl Pct Recovery = 103% Analysis Date = 02/01/17 SpikeMix = Supelco LC20140V: 30 µl & Abs 052616: 30 µl Pct Recovery = 94% Analysis Date = 01/13/17 SpikeMix = Abs 052616: 30 µl & ChemService 5016200: 30 µl Pct Recovery = 94% Analysis Date = 12/29/16 SpikeMix = ChemService 5016100: 30 µl & Abs 052616: 30 µl Pct Recovery = 89% Analysis Date = 03/07/16 SpikeMix = Abs 041515: 50 µl & ERA 0601-15-04: 50 µl Pct Recovery = 85% Analysis Date = 12/10/15 SpikeMix = Abs 041515: 50 µl & ERA 0601-15-04: 50 µl Pct Recovery = 83% Analysis Date = 08/17/15 SpikeMix = ChemService 4073900: 50 µl & Abs 041515: 50 µl Pct Recovery = 96% Analysis Date = 06/24/16 SpikeMix = Crescent 04EE007: 50 µl & Spex Organics EN150501025: 50 µl Pct Recovery = 85% Analysis Date = 01/08/16 SpikeMix = Crescent 04EE007: 50 µl & Spex Organics EN150501025: 50 µl Pct Recovery = 89% Analysis Date = 09/16/16 SpikeMix = Spex Organics EN160621015: 30 µl & ChemService 5016200: 30 µl Pct Recovery = 81% Analysis Date = 09/15/16 SpikeMix = Supelco LC20140V: 30 µl & Spex Organics EN160621015: 30 µl Pct Recovery = 61% Analysis Date = 04/01/15 SpikeMix = ChemService 2561700: 30 µl & Spex Organics E1140505004: 30 µl Pct Recovery = 108% Analysis Date = 01/21/15 SpikeMix = Supelco LC06946: 30 µl & ChemService 2561700: 30 µl Pct Recovery = 108% Analysis Date = 07/28/14 SpikeMix = ERA 0227-14-07.2: 30 µl & ChemService 2561700: 30 µl Pct Recovery = 125% Analysis Date = 05/14/14 SpikeMix = Abs 031014: 30 µl & ChemService 2561700: 30 µl Pct Recovery = 117% Analysis Date = 12/22/14 SpikeMix = Abs 042114: 30 µl & Abs 031014: 30 µl Pct Recovery = 74% Analysis Date = 12/16/14 SpikeMix = Supelco LC06946: 30 µl & Abs 042114: 30 µl Pct Recovery = 85% Analysis Date = 11/05/14 SpikeMix = ERA 0227-14-07.2: 30 µl & Abs 042114: 30 µl Pct Recovery = 78% Analysis Date = 03/07/16 SpikeMix = ChemService 4073900: 30 µl & Abs 041515: 30 µl Pct Recovery = 99% Analysis Date = 09/23/15 SpikeMix = ChemService 4073900: 30 µl & Spex Organics EN150501025: 30 µl Pct Recovery = 43% Analysis Date = 02/01/17 Pct Recovery = 79% Analysis Date = 01/21/17 Pct Recovery = 79% Analysis Date = 01/21/17 Pct Recovery = 79% Analysis Date = 01/10/17 Pct Recovery = 79% Analysis Date = 01/10/17 Pct Recovery = 79% Analysis Date = 12/30/16 Pct Recovery = 79% Analysis Date = 12/30/16 Pct Recovery = 79% Analysis Date = 12/19/16 Pct Recovery = 80% Analysis Date = 12/19/16 Pct Recovery = 80% Analysis Date = 12/09/16 Pct Recovery = 80% Analysis Date = 12/09/16 Pct Recovery = 80% Analysis Date = 11/28/16 Pct Recovery = 80% Analysis Date = 11/28/16 Pct Recovery = 80% Analysis Date = 11/17/16 Pct Recovery = 80% Analysis Date = 11/17/16 Pct Recovery = 80% Analysis Date = 11/06/16 Pct Recovery = 80% Analysis Date = 11/06/16 Pct Recovery = 80% Analysis Date = 10/27/16 Pct Recovery = 80% Analysis Date = 10/27/16 Pct Recovery = 80% Analysis Date = 10/16/16 Pct Recovery = 81% Analysis Date = 10/16/16 Pct Recovery = 81% Analysis Date = 10/05/16 Pct Recovery = 81% Analysis Date = 10/05/16 Pct Recovery = 81% Analysis Date = 09/24/16 Pct Recovery = 81% Analysis Date = 09/24/16 Pct Recovery = 81% Analysis Date = 09/13/16 Pct Recovery = 81% Analysis Date = 09/13/16 Pct Recovery = 81% Analysis Date = 09/03/16 Pct Recovery = 81% Analysis Date = 09/03/16 Pct Recovery = 81% Analysis Date = 08/23/16 Pct Recovery = 81% Analysis Date = 08/23/16 Pct Recovery = 81% Analysis Date = 08/12/16 Pct Recovery = 82% Analysis Date = 08/12/16 Pct Recovery = 82% Analysis Date = 08/01/16 Pct Recovery = 82% Analysis Date = 08/01/16 Pct Recovery = 82% Analysis Date = 07/22/16 Pct Recovery = 82% Analysis Date = 07/22/16 Pct Recovery = 82% Analysis Date = 07/11/16 Pct Recovery = 82% Analysis Date = 07/11/16 Pct Recovery = 82% Analysis Date = 06/30/16 Pct Recovery = 82% Analysis Date = 06/30/16 Pct Recovery = 82% Analysis Date = 06/19/16 Pct Recovery = 82% Analysis Date = 06/19/16 Pct Recovery = 82% Analysis Date = 06/08/16 Pct Recovery = 83% Analysis Date = 06/08/16 Pct Recovery = 83% Analysis Date = 05/29/16 Pct Recovery = 83% Analysis Date = 05/29/16 Pct Recovery = 83% Analysis Date = 05/18/16 Pct Recovery = 83% Analysis Date = 05/18/16 Pct Recovery = 83% Analysis Date = 05/07/16 Pct Recovery = 83% Analysis Date = 05/07/16 Pct Recovery = 83% Analysis Date = 04/26/16 Pct Recovery = 83% Analysis Date = 04/26/16 Pct Recovery = 83% Analysis Date = 04/16/16 Pct Recovery = 83% Analysis Date = 04/16/16 Pct Recovery = 83% Analysis Date = 04/05/16 Pct Recovery = 84% Analysis Date = 04/05/16 Pct Recovery = 84% Analysis Date = 03/25/16 Pct Recovery = 84% Analysis Date = 03/25/16 Pct Recovery = 84% Analysis Date = 03/14/16 Pct Recovery = 84% Analysis Date = 03/14/16 Pct Recovery = 84% Analysis Date = 03/03/16 Pct Recovery = 84% Analysis Date = 03/03/16 Pct Recovery = 84% Analysis Date = 02/22/16 Pct Recovery = 84% Analysis Date = 02/22/16 Pct Recovery = 84% Analysis Date = 02/11/16 Pct Recovery = 84% Analysis Date = 02/11/16 Pct Recovery = 84% Analysis Date = 01/31/16 Pct Recovery = 85% Analysis Date = 01/31/16 Pct Recovery = 85% Analysis Date = 01/20/16 Pct Recovery = 85% Analysis Date = 01/20/16 Pct Recovery = 85% Analysis Date = 01/10/16 Pct Recovery = 85% Analysis Date = 01/10/16 Pct Recovery = 85% Analysis Date = 12/30/15 Pct Recovery = 85% Analysis Date = 12/30/15 Pct Recovery = 85% Analysis Date = 12/19/15 Pct Recovery = 85% Analysis Date = 12/19/15 Pct Recovery = 85% Analysis Date = 12/08/15 Pct Recovery = 86% Analysis Date = 12/08/15 Pct Recovery = 86% Analysis Date = 11/28/15 Pct Recovery = 86% Analysis Date = 11/28/15 Pct Recovery = 86% Analysis Date = 11/17/15 Pct Recovery = 86% Analysis Date = 11/17/15 Pct Recovery = 86% Analysis Date = 11/06/15 Pct Recovery = 86% Analysis Date = 11/06/15 Pct Recovery = 86% Analysis Date = 10/26/15 Pct Recovery = 86% Analysis Date = 10/26/15 Pct Recovery = 86% Analysis Date = 10/15/15 Pct Recovery = 86% Analysis Date = 10/15/15 Pct Recovery = 86% Analysis Date = 10/05/15 Pct Recovery = 87% Analysis Date = 10/05/15 Pct Recovery = 87% Analysis Date = 09/24/15 Pct Recovery = 87% Analysis Date = 09/24/15 Pct Recovery = 87% Analysis Date = 09/13/15 Pct Recovery = 87% Analysis Date = 09/13/15 Pct Recovery = 87% Analysis Date = 09/02/15 Pct Recovery = 87% Analysis Date = 09/02/15 Pct Recovery = 87% Analysis Date = 08/23/15 Pct Recovery = 87% Analysis Date = 08/23/15 Pct Recovery = 87% Analysis Date = 08/12/15 Pct Recovery = 88% Analysis Date = 08/12/15 Pct Recovery = 88% Analysis Date = 08/01/15 Pct Recovery = 88% Analysis Date = 08/01/15 Pct Recovery = 88% Analysis Date = 07/21/15 Pct Recovery = 88% Analysis Date = 07/21/15 Pct Recovery = 88% Analysis Date = 07/10/15 Pct Recovery = 88% Analysis Date = 07/10/15 Pct Recovery = 88% Analysis Date = 06/30/15 Pct Recovery = 88% Analysis Date = 06/30/15 Pct Recovery = 88% Analysis Date = 06/19/15 Pct Recovery = 88% Analysis Date = 06/19/15 Pct Recovery = 88% Analysis Date = 06/08/15 Pct Recovery = 89% Analysis Date = 06/08/15 Pct Recovery = 89% Analysis Date = 05/28/15 Pct Recovery = 89% Analysis Date = 05/28/15 Pct Recovery = 89% Analysis Date = 05/18/15 Pct Recovery = 89% Analysis Date = 05/18/15 Pct Recovery = 89% Analysis Date = 05/07/15 Pct Recovery = 89% Analysis Date = 05/07/15 Pct Recovery = 89% Analysis Date = 04/26/15 Pct Recovery = 89% Analysis Date = 04/26/15 Pct Recovery = 89% Analysis Date = 04/15/15 Pct Recovery = 90% Analysis Date = 04/15/15 Pct Recovery = 90% Analysis Date = 04/04/15 Pct Recovery = 90% Analysis Date = 04/04/15 Pct Recovery = 90% Analysis Date = 03/25/15 Pct Recovery = 90% Analysis Date = 03/25/15 Pct Recovery = 90% Analysis Date = 03/14/15 Pct Recovery = 90% Analysis Date = 03/14/15 Pct Recovery = 90% Analysis Date = 03/03/15 Pct Recovery = 90% Analysis Date = 03/03/15 Pct Recovery = 90% Analysis Date = 02/20/15 Pct Recovery = 90% Analysis Date = 02/20/15 Pct Recovery = 90% Analysis Date = 02/10/15 Pct Recovery = 90% Analysis Date = 02/10/15 Pct Recovery = 90% Analysis Date = 01/30/15 Pct Recovery = 90% Analysis Date = 01/30/15 Pct Recovery = 90% Analysis Date = 01/19/15 Pct Recovery = 90% Analysis Date = 01/19/15 Pct Recovery = 90% Analysis Date = 01/08/15 Pct Recovery = 90% Analysis Date = 01/08/15 Pct Recovery = 90% Analysis Date = 12/28/14 Pct Recovery = 90% Analysis Date = 12/28/14 Pct Recovery = 90% Analysis Date = 12/18/14 Pct Recovery = 90% Analysis Date = 12/18/14 Pct Recovery = 90% Analysis Date = 12/07/14 Pct Recovery = 90% Analysis Date = 12/07/14 Pct Recovery = 90% Analysis Date = 11/26/14 Pct Recovery = 90% Analysis Date = 11/26/14 Pct Recovery = 90% Analysis Date = 11/15/14 Pct Recovery = 90% Analysis Date = 11/15/14 Pct Recovery = 90% Analysis Date = 11/05/14 Pct Recovery = 90% Analysis Date = 11/05/14 Pct Recovery = 90% Analysis Date = 10/25/14 Pct Recovery = 90% Analysis Date = 10/25/14 Pct Recovery = 90% Analysis Date = 10/14/14 Pct Recovery = 90% Analysis Date = 10/14/14 Pct Recovery = 90% Analysis Date = 10/03/14 Pct Recovery = 90% Analysis Date = 10/03/14 Pct Recovery = 90% Analysis Date = 09/23/14 Pct Recovery = 90% Analysis Date = 09/23/14 Pct Recovery = 90% Analysis Date = 09/12/14 Pct Recovery = 90% Analysis Date = 09/12/14 Pct Recovery = 90% Analysis Date = 09/01/14 Pct Recovery = 90% Analysis Date = 09/01/14 Pct Recovery = 90% Analysis Date = 08/21/14 Pct Recovery = 89% Analysis Date = 08/21/14 Pct Recovery = 89% Analysis Date = 08/10/14 Pct Recovery = 89% Analysis Date = 08/10/14 Pct Recovery = 89% Analysis Date = 07/31/14 Pct Recovery = 89% Analysis Date = 07/31/14 Pct Recovery = 89% Analysis Date = 07/20/14 Pct Recovery = 89% Analysis Date = 07/20/14 Pct Recovery = 89% Analysis Date = 07/09/14 Pct Recovery = 89% Analysis Date = 07/09/14 Pct Recovery = 89% Analysis Date = 06/28/14 Pct Recovery = 89% Analysis Date = 06/28/14 Pct Recovery = 89% Analysis Date = 06/18/14 Pct Recovery = 88% Analysis Date = 06/18/14 Pct Recovery = 88% Analysis Date = 06/07/14 Pct Recovery = 88% Analysis Date = 06/07/14 Pct Recovery = 88% Analysis Date = 05/27/14 Pct Recovery = 88% Analysis Date = 05/27/14 Pct Recovery = 88% Analysis Date = 05/16/14 Pct Recovery = 88% Analysis Date = 05/16/14 Pct Recovery = 88% Analysis Date = 05/05/14 Pct Recovery = 88% Analysis Date = 05/05/14 Pct Recovery = 88% Analysis Date = 04/25/14 Pct Recovery = 88% Analysis Date = 04/25/14 Pct Recovery = 88% Analysis Date = 04/14/14 Pct Recovery = 87% Analysis Date = 04/14/14 Pct Recovery = 87% Analysis Date = 04/03/14 Pct Recovery = 87% Analysis Date = 04/03/14 Pct Recovery = 87% Analysis Date = 03/23/14 Pct Recovery = 87% Analysis Date = 03/23/14 Pct Recovery = 87% Analysis Date = 03/13/14 Pct Recovery = 87% Analysis Date = 03/13/14 Pct Recovery = 87% Analysis Date = 03/02/14 Pct Recovery = 86% Analysis Date = 03/02/14 Pct Recovery = 86% Analysis Date = 02/19/14 Pct Recovery = 86% Analysis Date = 02/19/14 Pct Recovery = 86% Analysis Date = 02/08/14 Pct Recovery = 86% Analysis Date = 02/08/14 Pct Recovery = 86% Analysis Date = 01/28/14 Pct Recovery = 86% Analysis Date = 01/28/14 Pct Recovery = 86% Analysis Date = 01/18/14 Pct Recovery = 86% Analysis Date = 01/18/14 Pct Recovery = 86% Analysis Date = 01/07/14 Pct Recovery = 86% Analysis Date = 01/07/14 Pct Recovery = 86% Analysis Date = 12/27/13 Pct Recovery = 85% Analysis Date = 12/27/13 Pct Recovery = 85% Analysis Date = 12/16/13 Pct Recovery = 85% Analysis Date = 12/16/13 Pct Recovery = 85% Analysis Date = 12/06/13 Pct Recovery = 85% Analysis Date = 12/06/13 Pct Recovery = 85% Analysis Date = 11/25/13 Pct Recovery = 85% Analysis Date = 11/25/13 Pct Recovery = 85% Analysis Date = 11/14/13 Pct Recovery = 85% Analysis Date = 11/14/13 Pct Recovery = 85% Analysis Date = 11/03/13 Pct Recovery = 85% Analysis Date = 11/03/13 Pct Recovery = 85% Analysis Date = 10/23/13 Pct Recovery = 85% Analysis Date = 10/23/13 Pct Recovery = 85% Analysis Date = 10/13/13 Pct Recovery = 84% Analysis Date = 10/13/13 Pct Recovery = 84% Analysis Date = 10/02/13 Pct Recovery = 84% Analysis Date = 10/02/13 Pct Recovery = 84% Analysis Date = 09/21/13 Pct Recovery = 84% Analysis Date = 09/21/13 Pct Recovery = 84% Analysis Date = 09/10/13 Pct Recovery = 84% Analysis Date = 09/10/13 Pct Recovery = 84% Analysis Date = 08/31/13 Pct Recovery = 84% Analysis Date = 08/31/13 Pct Recovery = 84% Analysis Date = 08/20/13 Pct Recovery = 84% Analysis Date = 08/20/13 Pct Recovery = 84% Analysis Date = 08/09/13 Pct Recovery = 84% Analysis Date = 08/09/13 Pct Recovery = 84% Analysis Date = 07/29/13 Pct Recovery = 83% Analysis Date = 07/29/13 Pct Recovery = 83% Analysis Date = 07/19/13 Pct Recovery = 83% Analysis Date = 07/19/13 Pct Recovery = 83% Analysis Date = 07/08/13 Pct Recovery = 83% Analysis Date = 07/08/13 Pct Recovery = 83% Analysis Date = 06/27/13 Pct Recovery = 83% Analysis Date = 06/27/13 Pct Recovery = 83% Analysis Date = 06/16/13 Pct Recovery = 83% Analysis Date = 06/16/13 Pct Recovery = 83% Analysis Date = 06/05/13 Pct Recovery = 83% Analysis Date = 06/05/13 Pct Recovery = 83% Analysis Date = 05/26/13 Pct Recovery = 82% Analysis Date = 05/26/13 Pct Recovery = 82% Analysis Date = 05/15/13 Pct Recovery = 82% Analysis Date = 05/15/13 Pct Recovery = 82% Analysis Date = 05/04/13 Pct Recovery = 82% Analysis Date = 05/04/13 Pct Recovery = 82% Analysis Date = 04/23/13 Pct Recovery = 82% Analysis Date = 04/23/13 Pct Recovery = 82% Analysis Date = 04/13/13 Pct Recovery = 82% Analysis Date = 04/13/13 Pct Recovery = 82% Analysis Date = 04/02/13 Pct Recovery = 82% Analysis Date = 04/02/13 Pct Recovery = 82% Analysis Date = 03/22/13 Pct Recovery = 82% Analysis Date = 03/22/13 Pct Recovery = 82% Analysis Date = 03/11/13 Pct Recovery = 82% Analysis Date = 03/11/13 Pct Recovery = 82% Analysis Date = 02/28/13 Pct Recovery = 82% Analysis Date = 02/28/13 Pct Recovery = 82% Analysis Date = 02/18/13 Pct Recovery = 82% Analysis Date = 02/18/13 Pct Recovery = 82% Analysis Date = 02/07/13 Pct Recovery = 82% Analysis Date = 02/07/13 Pct Recovery = 82% Analysis Date = 01/27/13 Pct Recovery = 82% Analysis Date = 01/27/13 Pct Recovery = 82% Analysis Date = 01/16/13 Pct Recovery = 82% Analysis Date = 01/16/13 Pct Recovery = 82% Analysis Date = 01/06/13 Pct Recovery = 82% Analysis Date = 01/06/13 Pct Recovery = 82% Analysis Date = 12/26/12 Pct Recovery = 82% Analysis Date = 12/26/12 Pct Recovery = 82% Analysis Date = 12/15/12 Pct Recovery = 82% Analysis Date = 12/15/12 Pct Recovery = 82% Analysis Date = 12/04/12 Pct Recovery = 82% Analysis Date = 12/04/12 Pct Recovery = 82% Analysis Date = 11/23/12 Pct Recovery = 82% Analysis Date = 11/23/12 Pct Recovery = 82% Analysis Date = 11/13/12 Pct Recovery = 82% Analysis Date = 11/13/12 Pct Recovery = 82% Analysis Date = 11/02/12 Pct Recovery = 82% Analysis Date = 11/02/12 Pct Recovery = 82% Analysis Date = 10/22/12 Pct Recovery = 82% Analysis Date = 10/22/12 Pct Recovery = 82% Analysis Date = 10/11/12 Pct Recovery = 83% Analysis Date = 10/11/12 Pct Recovery = 83% Analysis Date = 10/01/12 Pct Recovery = 83% Analysis Date = 10/01/12 Pct Recovery = 83% Analysis Date = 09/20/12 Pct Recovery = 83% Analysis Date = 09/20/12 Pct Recovery = 83% Analysis Date = 09/09/12 Pct Recovery = 83% Analysis Date = 09/09/12 Pct Recovery = 83% Analysis Date = 08/29/12 Pct Recovery = 83% Analysis Date = 08/29/12 Pct Recovery = 83% Analysis Date = 08/18/12 Pct Recovery = 83% Analysis Date = 08/18/12 Pct Recovery = 83% Analysis Date = 08/08/12 Pct Recovery = 83% Analysis Date = 08/08/12 Pct Recovery = 83% Analysis Date = 07/28/12 Pct Recovery = 83% Analysis Date = 07/28/12 Pct Recovery = 83% Analysis Date = 07/17/12 Pct Recovery = 83% Analysis Date = 07/17/12 Pct Recovery = 83% Analysis Date = 07/06/12 Pct Recovery = 83% Analysis Date = 07/06/12 Pct Recovery = 83% Analysis Date = 06/26/12 Pct Recovery = 83% Analysis Date = 06/26/12 Pct Recovery = 83% Analysis Date = 06/15/12 Pct Recovery = 83% Analysis Date = 06/15/12 Pct Recovery = 83% Analysis Date = 06/04/12 Pct Recovery = 83% Analysis Date = 06/04/12 Pct Recovery = 83% Analysis Date = 05/24/12 Pct Recovery = 83% Analysis Date = 05/24/12 Pct Recovery = 83% Analysis Date = 05/14/12 Pct Recovery = 83% Analysis Date = 05/14/12 Pct Recovery = 83% Analysis Date = 05/03/12 Pct Recovery = 83% Analysis Date = 05/03/12 Pct Recovery = 83% Analysis Date = 04/22/12 Pct Recovery = 83% Analysis Date = 04/22/12 Pct Recovery = 83% Analysis Date = 04/11/12 Pct Recovery = 83% Analysis Date = 04/11/12 Pct Recovery = 83% Analysis Date = 03/31/12 Pct Recovery = 84% Analysis Date = 03/31/12 Pct Recovery = 84% Analysis Date = 03/21/12 Pct Recovery = 84% Analysis Date = 03/21/12 Pct Recovery = 84% Analysis Date = 03/10/12 Pct Recovery = 84% Analysis Date = 03/10/12 Pct Recovery = 84% Analysis Date = 02/28/12 Pct Recovery = 84% Analysis Date = 02/28/12 Pct Recovery = 84% Analysis Date = 02/17/12 Pct Recovery = 84% Analysis Date = 02/17/12 Pct Recovery = 84% Analysis Date = 02/07/12 Pct Recovery = 84% Analysis Date = 02/07/12 Pct Recovery = 84% Analysis Date = 01/27/12 Pct Recovery = 84% Analysis Date = 01/27/12 Pct Recovery = 84% Analysis Date = 01/16/12 Pct Recovery = 84% Analysis Date = 01/16/12 Pct Recovery = 84% Analysis Date = 01/05/12 Pct Recovery = 84% Analysis Date = 01/05/12 Pct Recovery = 84% Analysis Date = 12/25/11 Pct Recovery = 84% Analysis Date = 12/25/11 Pct Recovery = 84% Analysis Date = 12/15/11 Pct Recovery = 84% Analysis Date = 12/15/11 Pct Recovery = 84% Analysis Date = 12/04/11 Pct Recovery = 84% Analysis Date = 12/04/11 Pct Recovery = 84% Analysis Date = 11/23/11 Pct Recovery = 84% Analysis Date = 11/23/11 Pct Recovery = 84% Analysis Date = 11/12/11 Pct Recovery = 84% Analysis Date = 11/12/11 Pct Recovery = 84% Analysis Date = 11/02/11 Pct Recovery = 84% Analysis Date = 11/02/11 Pct Recovery = 84% Analysis Date = 10/22/11 Pct Recovery = 84% Analysis Date = 10/22/11 Pct Recovery = 84% Analysis Date = 10/11/11 Pct Recovery = 84% Analysis Date = 10/11/11 Pct Recovery = 84% Analysis Date = 09/30/11 Pct Recovery = 84% Analysis Date = 09/30/11 Pct Recovery = 84% Analysis Date = 09/19/11 Pct Recovery = 84% Analysis Date = 09/19/11 Pct Recovery = 84% Analysis Date = 09/09/11 Pct Recovery = 84% Analysis Date = 09/09/11 Pct Recovery = 84% Analysis Date = 08/29/11 Pct Recovery = 84% Analysis Date = 08/29/11 Pct Recovery = 84% Analysis Date = 08/18/11 Pct Recovery = 84% Analysis Date = 08/18/11 Pct Recovery = 84% Analysis Date = 08/07/11 Pct Recovery = 84% Analysis Date = 08/07/11 Pct Recovery = 84% Analysis Date = 07/28/11 Pct Recovery = 84% Analysis Date = 07/28/11 Pct Recovery = 84% Analysis Date = 07/17/11 Pct Recovery = 84% Analysis Date = 07/17/11 Pct Recovery = 84% Analysis Date = 07/06/11 Pct Recovery = 84% Analysis Date = 07/06/11 Pct Recovery = 84% Analysis Date = 06/25/11 Pct Recovery = 85% Analysis Date = 06/25/11 Pct Recovery = 85% Analysis Date = 06/14/11 Pct Recovery = 85% Analysis Date = 06/14/11 Pct Recovery = 85% Analysis Date = 06/04/11 Pct Recovery = 85% Analysis Date = 06/04/11 Pct Recovery = 85% Analysis Date = 05/24/11 Pct Recovery = 85% Analysis Date = 05/24/11 Pct Recovery = 85% Analysis Date = 05/13/11 Pct Recovery = 85% Analysis Date = 05/13/11 Pct Recovery = 85% Analysis Date = 05/02/11 Pct Recovery = 85% Analysis Date = 05/02/11 Pct Recovery = 85% Analysis Date = 04/22/11 Pct Recovery = 85% Analysis Date = 04/22/11 Pct Recovery = 85% Analysis Date = 04/11/11 Pct Recovery = 85% Analysis Date = 04/11/11 Pct Recovery = 85% Analysis Date = 03/31/11 Pct Recovery = 85% Analysis Date = 03/31/11 Pct Recovery = 85% Analysis Date = 03/20/11 Pct Recovery = 85% Analysis Date = 03/20/11 Pct Recovery = 85% Analysis Date = 03/10/11 Pct Recovery = 85% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
17-BETA-ESTRADIOL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 69 85% 17% 83% 12%
Total 69 85% 17% 83% 12%

Sample Statistics
17-BETA-ESTRADIOL

Characteristic N % % Basis
Plotted 69 86% Spiked
Estimated Values 0 0% Spiked
Deleted Values 2 2% Spiked + Not Spiked
Spiked, Censored 1 1% Spiked
Spiked 82 .  
False Negatives 10 13% 10 out of 80
Not Spiked 49 .  
False Positives 0 0% 0 out of 49

BQS OBSP Determination:
3-BETA-COPROSTANOL
METHOD: 4434 , TESTIDCODE: 64532GM005
Open Data Set

Analysis Date = 05/09/11 SpikeMix = Abs 081810: 100 µl Pct Recovery = 77% Analysis Date = 07/02/12 SpikeMix = Abs 081810: 100 µl Pct Recovery = 121% Analysis Date = 04/17/12 SpikeMix = Abs 081810: 100 µl Pct Recovery = 128% Analysis Date = 10/03/11 SpikeMix = Abs 081810: 100 µl Pct Recovery = 82% Analysis Date = 02/01/12 SpikeMix = Spex Organics T1100629008: 100 µl Pct Recovery = 93% Analysis Date = 09/29/11 SpikeMix = Spex Organics T1100629008: 100 µl Pct Recovery = 78% Analysis Date = 03/31/11 SpikeMix = Spex Organics T1100629008: 100 µl Pct Recovery = 80% Analysis Date = 12/03/12 SpikeMix = ERA 0511-12-02: 50 µl & Abs 051512: 50 µl Pct Recovery = 119% Analysis Date = 02/22/13 SpikeMix = Restek A089631: 50 µl & Supelco LB92781: 50 µl Pct Recovery = 93% Analysis Date = 12/18/12 SpikeMix = Spex Organics T1120525010: 50 µl & Supelco LB92781: 50 µl Pct Recovery = 98% Analysis Date = 04/03/13 SpikeMix = Spex Organics T1120525010: 25 µl & Abs 051512: 25 µl Pct Recovery = 94% Analysis Date = 11/01/12 SpikeMix = ERA 0507-12-04.1: 25 µl & Abs 051512: 25 µl Pct Recovery = 121% Analysis Date = 08/31/12 SpikeMix = ERA 0511-12-02: 25 µl & Abs 051512: 25 µl Pct Recovery = 124% Analysis Date = 08/24/12 SpikeMix = Abs 051512: 25 µl Pct Recovery = 139% Analysis Date = 04/10/13 SpikeMix = ERA 0511-12-02: 25 µl & Supelco LB92781: 25 µl Pct Recovery = 89% Analysis Date = 02/08/13 SpikeMix = ERA 0507-12-04.1: 25 µl & Supelco LB92781: 25 µl Pct Recovery = 129% Analysis Date = 12/18/12 SpikeMix = Restek A089631: 25 µl & Supelco LB92781: 25 µl Pct Recovery = 96% Analysis Date = 05/26/11 SpikeMix = Spex Organics T1100629008: 25 µl Pct Recovery = 97% Analysis Date = 03/27/12 SpikeMix = Abs 081810: 25 µl Pct Recovery = 119% Analysis Date = 01/27/12 SpikeMix = Abs 081810: 25 µl Pct Recovery = 136% Analysis Date = 10/12/11 SpikeMix = Abs 081810: 25 µl Pct Recovery = 92% Analysis Date = 08/16/12 SpikeMix = Spex Organics T1100629008: 25 µl Pct Recovery = 138% Analysis Date = 11/28/11 SpikeMix = Spex Organics T1100629008: 25 µl Pct Recovery = 91% Analysis Date = 10/13/11 SpikeMix = Spex Organics T1100629008: 25 µl Pct Recovery = 105% Analysis Date = 03/10/11 SpikeMix = Spex Organics T1100629008: 25 µl Pct Recovery = 87% Analysis Date = 06/13/11 SpikeMix = Abs 081810: 25 µl Pct Recovery = 97% Analysis Date = 03/30/11 SpikeMix = Abs 081810: 25 µl Pct Recovery = 75% Analysis Date = 07/11/11 SpikeMix = Spex Organics T1100629008: 25 µl Pct Recovery = 86% Analysis Date = 03/14/14 SpikeMix = Supelco LB99393: 50 µl & Abs 050813: 50 µl Pct Recovery = 68% Analysis Date = 02/25/14 SpikeMix = ERA 0415-13-01.1A: 50 µl & Abs 050813: 50 µl Pct Recovery = 85% Analysis Date = 03/05/14 SpikeMix = Spex Organics T1130423008: 50 µl & Abs 071513: 50 µl Pct Recovery = 60% Analysis Date = 08/09/13 SpikeMix = ERA 0415-13-01.2A: 50 µl & Spex Organics T1130423008: 50 µl Pct Recovery = 59% Analysis Date = 12/15/16 SpikeMix = Abs 061416H: 50 µl & ChemService 5016100: 50 µl Pct Recovery = 46% Analysis Date = 08/19/16 SpikeMix = Supelco LC20140V: 50 µl & Spex Organics TS160420010: 50 µl Pct Recovery = 43% Analysis Date = 08/11/16 SpikeMix = ChemService 5016100: 50 µl & Spex Organics TS160420010: 50 µl Pct Recovery = 56% Analysis Date = 12/09/14 SpikeMix = Abs 031014: 60 µl & Supelco LC06946: 60 µl Pct Recovery = 62% Analysis Date = 08/26/14 SpikeMix = Abs 031014: 60 µl & Abs 042114: 60 µl Pct Recovery = 60% Analysis Date = 08/11/14 SpikeMix = Abs 031014: 60 µl & ERA 0227-14-07.2: 60 µl Pct Recovery = 60% Analysis Date = 05/06/14 SpikeMix = Abs 031014: 60 µl & ChemService 2561700: 60 µl Pct Recovery = 89% Analysis Date = 04/13/15 SpikeMix = Abs 042114: 60 µl & Spex Organics E1140505004: 60 µl Pct Recovery = 60% Analysis Date = 04/01/15 SpikeMix = Spex Organics E1140505004: 60 µl & Supelco LC06946: 60 µl Pct Recovery = 47% Analysis Date = 01/21/15 SpikeMix = ChemService 2561700: 60 µl & Spex Organics E1140505004: 60 µl Pct Recovery = 53% Analysis Date = 01/08/16 SpikeMix = Spex Organics EN150501025: 60 µl & ERA 0601-15-04: 60 µl Pct Recovery = 51% Analysis Date = 01/07/16 SpikeMix = Crescent 04EE007: 60 µl & Abs 041515: 60 µl Pct Recovery = 73% Analysis Date = 09/15/16 SpikeMix = Supelco LC20140V: 30 µl & Spex Organics EN160621015: 30 µl Pct Recovery = 45% Analysis Date = 09/09/16 SpikeMix = ChemService 5016200: 30 µl & Supelco LC20140V: 30 µl Pct Recovery = 45% Analysis Date = 07/12/16 SpikeMix = Spex Organics EN150501025: 50 µl & ERA 0601-15-04: 50 µl Pct Recovery = 74% Analysis Date = 06/24/16 SpikeMix = Crescent 04EE007: 50 µl & Spex Organics EN150501025: 50 µl Pct Recovery = 54% Analysis Date = 01/08/16 SpikeMix = Crescent 04EE007: 50 µl & Spex Organics EN150501025: 50 µl Pct Recovery = 56% Analysis Date = 03/07/16 SpikeMix = Abs 041515: 50 µl & ERA 0601-15-04: 50 µl Pct Recovery = 57% Analysis Date = 12/10/15 SpikeMix = Abs 041515: 50 µl & ERA 0601-15-04: 50 µl Pct Recovery = 51% Analysis Date = 06/03/15 SpikeMix = Abs 031014: 30 µl & ERA 0227-14-07.2: 30 µl Pct Recovery = 66% Analysis Date = 12/22/14 SpikeMix = Abs 042114: 30 µl & Abs 031014: 30 µl Pct Recovery = 96% Analysis Date = 07/14/14 SpikeMix = ERA 0227-14-07.2: 30 µl & Abs 031014: 30 µl Pct Recovery = 56% Analysis Date = 05/14/14 SpikeMix = Abs 031014: 30 µl & ChemService 2561700: 30 µl Pct Recovery = 67% Analysis Date = 04/01/15 SpikeMix = ChemService 2561700: 30 µl & Spex Organics E1140505004: 30 µl Pct Recovery = 62% Analysis Date = 12/23/14 SpikeMix = Spex Organics E1140505004: 30 µl & Supelco LC06946: 30 µl Pct Recovery = 51% Analysis Date = 02/19/14 SpikeMix = Abs 050813: 20 µl & Abs 071513: 20 µl Pct Recovery = 79% Analysis Date = 11/18/13 SpikeMix = ERA 0415-13-01.2A: 20 µl & Abs 050813: 20 µl Pct Recovery = 67% Analysis Date = 12/09/13 SpikeMix = Supelco LB99393: 20 µl & Spex Organics T1130423008: 20 µl Pct Recovery = 113% Analysis Date = 12/14/16 Pct Recovery = 49% Analysis Date = 12/04/16 Pct Recovery = 49% Analysis Date = 12/04/16 Pct Recovery = 49% Analysis Date = 11/23/16 Pct Recovery = 50% Analysis Date = 11/23/16 Pct Recovery = 50% Analysis Date = 11/13/16 Pct Recovery = 50% Analysis Date = 11/13/16 Pct Recovery = 50% Analysis Date = 11/02/16 Pct Recovery = 50% Analysis Date = 11/02/16 Pct Recovery = 50% Analysis Date = 10/23/16 Pct Recovery = 50% Analysis Date = 10/23/16 Pct Recovery = 50% Analysis Date = 10/12/16 Pct Recovery = 50% Analysis Date = 10/12/16 Pct Recovery = 50% Analysis Date = 10/02/16 Pct Recovery = 51% Analysis Date = 10/02/16 Pct Recovery = 51% Analysis Date = 09/21/16 Pct Recovery = 51% Analysis Date = 09/21/16 Pct Recovery = 51% Analysis Date = 09/11/16 Pct Recovery = 51% Analysis Date = 09/11/16 Pct Recovery = 51% Analysis Date = 08/31/16 Pct Recovery = 51% Analysis Date = 08/31/16 Pct Recovery = 51% Analysis Date = 08/21/16 Pct Recovery = 52% Analysis Date = 08/21/16 Pct Recovery = 52% Analysis Date = 08/10/16 Pct Recovery = 52% Analysis Date = 08/10/16 Pct Recovery = 52% Analysis Date = 07/31/16 Pct Recovery = 52% Analysis Date = 07/31/16 Pct Recovery = 52% Analysis Date = 07/20/16 Pct Recovery = 52% Analysis Date = 07/20/16 Pct Recovery = 52% Analysis Date = 07/09/16 Pct Recovery = 52% Analysis Date = 07/09/16 Pct Recovery = 52% Analysis Date = 06/29/16 Pct Recovery = 53% Analysis Date = 06/29/16 Pct Recovery = 53% Analysis Date = 06/18/16 Pct Recovery = 53% Analysis Date = 06/18/16 Pct Recovery = 53% Analysis Date = 06/08/16 Pct Recovery = 53% Analysis Date = 06/08/16 Pct Recovery = 53% Analysis Date = 05/28/16 Pct Recovery = 53% Analysis Date = 05/28/16 Pct Recovery = 53% Analysis Date = 05/18/16 Pct Recovery = 54% Analysis Date = 05/18/16 Pct Recovery = 54% Analysis Date = 05/07/16 Pct Recovery = 54% Analysis Date = 05/07/16 Pct Recovery = 54% Analysis Date = 04/27/16 Pct Recovery = 54% Analysis Date = 04/27/16 Pct Recovery = 54% Analysis Date = 04/16/16 Pct Recovery = 54% Analysis Date = 04/16/16 Pct Recovery = 54% Analysis Date = 04/06/16 Pct Recovery = 54% Analysis Date = 04/06/16 Pct Recovery = 54% Analysis Date = 03/26/16 Pct Recovery = 55% Analysis Date = 03/26/16 Pct Recovery = 55% Analysis Date = 03/16/16 Pct Recovery = 55% Analysis Date = 03/16/16 Pct Recovery = 55% Analysis Date = 03/05/16 Pct Recovery = 55% Analysis Date = 03/05/16 Pct Recovery = 55% Analysis Date = 02/24/16 Pct Recovery = 55% Analysis Date = 02/24/16 Pct Recovery = 55% Analysis Date = 02/13/16 Pct Recovery = 56% Analysis Date = 02/13/16 Pct Recovery = 56% Analysis Date = 02/02/16 Pct Recovery = 56% Analysis Date = 02/02/16 Pct Recovery = 56% Analysis Date = 01/23/16 Pct Recovery = 56% Analysis Date = 01/23/16 Pct Recovery = 56% Analysis Date = 01/12/16 Pct Recovery = 56% Analysis Date = 01/12/16 Pct Recovery = 56% Analysis Date = 01/02/16 Pct Recovery = 57% Analysis Date = 01/02/16 Pct Recovery = 57% Analysis Date = 12/22/15 Pct Recovery = 57% Analysis Date = 12/22/15 Pct Recovery = 57% Analysis Date = 12/12/15 Pct Recovery = 57% Analysis Date = 12/12/15 Pct Recovery = 57% Analysis Date = 12/01/15 Pct Recovery = 57% Analysis Date = 12/01/15 Pct Recovery = 57% Analysis Date = 11/21/15 Pct Recovery = 57% Analysis Date = 11/21/15 Pct Recovery = 57% Analysis Date = 11/10/15 Pct Recovery = 58% Analysis Date = 11/10/15 Pct Recovery = 58% Analysis Date = 10/31/15 Pct Recovery = 58% Analysis Date = 10/31/15 Pct Recovery = 58% Analysis Date = 10/20/15 Pct Recovery = 58% Analysis Date = 10/20/15 Pct Recovery = 58% Analysis Date = 10/10/15 Pct Recovery = 58% Analysis Date = 10/10/15 Pct Recovery = 58% Analysis Date = 09/29/15 Pct Recovery = 59% Analysis Date = 09/29/15 Pct Recovery = 59% Analysis Date = 09/18/15 Pct Recovery = 59% Analysis Date = 09/18/15 Pct Recovery = 59% Analysis Date = 09/08/15 Pct Recovery = 59% Analysis Date = 09/08/15 Pct Recovery = 59% Analysis Date = 08/28/15 Pct Recovery = 59% Analysis Date = 08/28/15 Pct Recovery = 59% Analysis Date = 08/18/15 Pct Recovery = 60% Analysis Date = 08/18/15 Pct Recovery = 60% Analysis Date = 08/07/15 Pct Recovery = 60% Analysis Date = 08/07/15 Pct Recovery = 60% Analysis Date = 07/28/15 Pct Recovery = 60% Analysis Date = 07/28/15 Pct Recovery = 60% Analysis Date = 07/17/15 Pct Recovery = 60% Analysis Date = 07/17/15 Pct Recovery = 60% Analysis Date = 07/07/15 Pct Recovery = 61% Analysis Date = 07/07/15 Pct Recovery = 61% Analysis Date = 06/26/15 Pct Recovery = 61% Analysis Date = 06/26/15 Pct Recovery = 61% Analysis Date = 06/16/15 Pct Recovery = 61% Analysis Date = 06/16/15 Pct Recovery = 61% Analysis Date = 06/05/15 Pct Recovery = 61% Analysis Date = 06/05/15 Pct Recovery = 61% Analysis Date = 05/26/15 Pct Recovery = 62% Analysis Date = 05/26/15 Pct Recovery = 62% Analysis Date = 05/15/15 Pct Recovery = 62% Analysis Date = 05/15/15 Pct Recovery = 62% Analysis Date = 05/05/15 Pct Recovery = 62% Analysis Date = 05/05/15 Pct Recovery = 62% Analysis Date = 04/24/15 Pct Recovery = 62% Analysis Date = 04/24/15 Pct Recovery = 62% Analysis Date = 04/13/15 Pct Recovery = 62% Analysis Date = 04/13/15 Pct Recovery = 62% Analysis Date = 04/03/15 Pct Recovery = 63% Analysis Date = 04/03/15 Pct Recovery = 63% Analysis Date = 03/23/15 Pct Recovery = 63% Analysis Date = 03/23/15 Pct Recovery = 63% Analysis Date = 03/13/15 Pct Recovery = 63% Analysis Date = 03/13/15 Pct Recovery = 63% Analysis Date = 03/02/15 Pct Recovery = 64% Analysis Date = 03/02/15 Pct Recovery = 64% Analysis Date = 02/20/15 Pct Recovery = 64% Analysis Date = 02/20/15 Pct Recovery = 64% Analysis Date = 02/09/15 Pct Recovery = 64% Analysis Date = 02/09/15 Pct Recovery = 64% Analysis Date = 01/30/15 Pct Recovery = 64% Analysis Date = 01/30/15 Pct Recovery = 64% Analysis Date = 01/19/15 Pct Recovery = 65% Analysis Date = 01/19/15 Pct Recovery = 65% Analysis Date = 01/09/15 Pct Recovery = 65% Analysis Date = 01/09/15 Pct Recovery = 65% Analysis Date = 12/29/14 Pct Recovery = 65% Analysis Date = 12/29/14 Pct Recovery = 65% Analysis Date = 12/19/14 Pct Recovery = 66% Analysis Date = 12/19/14 Pct Recovery = 66% Analysis Date = 12/08/14 Pct Recovery = 66% Analysis Date = 12/08/14 Pct Recovery = 66% Analysis Date = 11/28/14 Pct Recovery = 66% Analysis Date = 11/28/14 Pct Recovery = 66% Analysis Date = 11/17/14 Pct Recovery = 66% Analysis Date = 11/17/14 Pct Recovery = 66% Analysis Date = 11/06/14 Pct Recovery = 67% Analysis Date = 11/06/14 Pct Recovery = 67% Analysis Date = 10/27/14 Pct Recovery = 67% Analysis Date = 10/27/14 Pct Recovery = 67% Analysis Date = 10/16/14 Pct Recovery = 67% Analysis Date = 10/16/14 Pct Recovery = 67% Analysis Date = 10/06/14 Pct Recovery = 68% Analysis Date = 10/06/14 Pct Recovery = 68% Analysis Date = 09/25/14 Pct Recovery = 68% Analysis Date = 09/25/14 Pct Recovery = 68% Analysis Date = 09/15/14 Pct Recovery = 68% Analysis Date = 09/15/14 Pct Recovery = 68% Analysis Date = 09/04/14 Pct Recovery = 69% Analysis Date = 09/04/14 Pct Recovery = 69% Analysis Date = 08/25/14 Pct Recovery = 69% Analysis Date = 08/25/14 Pct Recovery = 69% Analysis Date = 08/14/14 Pct Recovery = 69% Analysis Date = 08/14/14 Pct Recovery = 69% Analysis Date = 08/04/14 Pct Recovery = 69% Analysis Date = 08/04/14 Pct Recovery = 69% Analysis Date = 07/24/14 Pct Recovery = 70% Analysis Date = 07/24/14 Pct Recovery = 70% Analysis Date = 07/14/14 Pct Recovery = 70% Analysis Date = 07/14/14 Pct Recovery = 70% Analysis Date = 07/03/14 Pct Recovery = 71% Analysis Date = 07/03/14 Pct Recovery = 71% Analysis Date = 06/22/14 Pct Recovery = 71% Analysis Date = 06/22/14 Pct Recovery = 71% Analysis Date = 06/12/14 Pct Recovery = 72% Analysis Date = 06/12/14 Pct Recovery = 72% Analysis Date = 06/01/14 Pct Recovery = 72% Analysis Date = 06/01/14 Pct Recovery = 72% Analysis Date = 05/22/14 Pct Recovery = 73% Analysis Date = 05/22/14 Pct Recovery = 73% Analysis Date = 05/11/14 Pct Recovery = 73% Analysis Date = 05/11/14 Pct Recovery = 73% Analysis Date = 05/01/14 Pct Recovery = 74% Analysis Date = 05/01/14 Pct Recovery = 74% Analysis Date = 04/20/14 Pct Recovery = 74% Analysis Date = 04/20/14 Pct Recovery = 74% Analysis Date = 04/10/14 Pct Recovery = 75% Analysis Date = 04/10/14 Pct Recovery = 75% Analysis Date = 03/30/14 Pct Recovery = 75% Analysis Date = 03/30/14 Pct Recovery = 75% Analysis Date = 03/20/14 Pct Recovery = 76% Analysis Date = 03/20/14 Pct Recovery = 76% Analysis Date = 03/09/14 Pct Recovery = 76% Analysis Date = 03/09/14 Pct Recovery = 76% Analysis Date = 02/27/14 Pct Recovery = 77% Analysis Date = 02/27/14 Pct Recovery = 77% Analysis Date = 02/16/14 Pct Recovery = 78% Analysis Date = 02/16/14 Pct Recovery = 78% Analysis Date = 02/06/14 Pct Recovery = 79% Analysis Date = 02/06/14 Pct Recovery = 79% Analysis Date = 01/26/14 Pct Recovery = 79% Analysis Date = 01/26/14 Pct Recovery = 79% Analysis Date = 01/15/14 Pct Recovery = 80% Analysis Date = 01/15/14 Pct Recovery = 80% Analysis Date = 01/05/14 Pct Recovery = 81% Analysis Date = 01/05/14 Pct Recovery = 81% Analysis Date = 12/25/13 Pct Recovery = 81% Analysis Date = 12/25/13 Pct Recovery = 81% Analysis Date = 12/15/13 Pct Recovery = 82% Analysis Date = 12/15/13 Pct Recovery = 82% Analysis Date = 12/04/13 Pct Recovery = 83% Analysis Date = 12/04/13 Pct Recovery = 83% Analysis Date = 11/24/13 Pct Recovery = 83% Analysis Date = 11/24/13 Pct Recovery = 83% Analysis Date = 11/13/13 Pct Recovery = 84% Analysis Date = 11/13/13 Pct Recovery = 84% Analysis Date = 11/03/13 Pct Recovery = 85% Analysis Date = 11/03/13 Pct Recovery = 85% Analysis Date = 10/23/13 Pct Recovery = 85% Analysis Date = 10/23/13 Pct Recovery = 85% Analysis Date = 10/13/13 Pct Recovery = 86% Analysis Date = 10/13/13 Pct Recovery = 86% Analysis Date = 10/02/13 Pct Recovery = 87% Analysis Date = 10/02/13 Pct Recovery = 87% Analysis Date = 09/22/13 Pct Recovery = 87% Analysis Date = 09/22/13 Pct Recovery = 87% Analysis Date = 09/11/13 Pct Recovery = 88% Analysis Date = 09/11/13 Pct Recovery = 88% Analysis Date = 09/01/13 Pct Recovery = 89% Analysis Date = 09/01/13 Pct Recovery = 89% Analysis Date = 08/21/13 Pct Recovery = 89% Analysis Date = 08/21/13 Pct Recovery = 89% Analysis Date = 08/10/13 Pct Recovery = 90% Analysis Date = 08/10/13 Pct Recovery = 90% Analysis Date = 07/31/13 Pct Recovery = 91% Analysis Date = 07/31/13 Pct Recovery = 91% Analysis Date = 07/20/13 Pct Recovery = 91% Analysis Date = 07/20/13 Pct Recovery = 91% Analysis Date = 07/10/13 Pct Recovery = 92% Analysis Date = 07/10/13 Pct Recovery = 92% Analysis Date = 06/29/13 Pct Recovery = 93% Analysis Date = 06/29/13 Pct Recovery = 93% Analysis Date = 06/19/13 Pct Recovery = 93% Analysis Date = 06/19/13 Pct Recovery = 93% Analysis Date = 06/08/13 Pct Recovery = 94% Analysis Date = 06/08/13 Pct Recovery = 94% Analysis Date = 05/29/13 Pct Recovery = 95% Analysis Date = 05/29/13 Pct Recovery = 95% Analysis Date = 05/18/13 Pct Recovery = 95% Analysis Date = 05/18/13 Pct Recovery = 95% Analysis Date = 05/08/13 Pct Recovery = 96% Analysis Date = 05/08/13 Pct Recovery = 96% Analysis Date = 04/27/13 Pct Recovery = 97% Analysis Date = 04/27/13 Pct Recovery = 97% Analysis Date = 04/17/13 Pct Recovery = 97% Analysis Date = 04/17/13 Pct Recovery = 97% Analysis Date = 04/06/13 Pct Recovery = 98% Analysis Date = 04/06/13 Pct Recovery = 98% Analysis Date = 03/26/13 Pct Recovery = 99% Analysis Date = 03/26/13 Pct Recovery = 99% Analysis Date = 03/16/13 Pct Recovery = 99% Analysis Date = 03/16/13 Pct Recovery = 99% Analysis Date = 03/05/13 Pct Recovery = 100% Analysis Date = 03/05/13 Pct Recovery = 100% Analysis Date = 02/23/13 Pct Recovery = 101% Analysis Date = 02/23/13 Pct Recovery = 101% Analysis Date = 02/12/13 Pct Recovery = 101% Analysis Date = 02/12/13 Pct Recovery = 101% Analysis Date = 02/02/13 Pct Recovery = 102% Analysis Date = 02/02/13 Pct Recovery = 102% Analysis Date = 01/22/13 Pct Recovery = 103% Analysis Date = 01/22/13 Pct Recovery = 103% Analysis Date = 01/12/13 Pct Recovery = 103% Analysis Date = 01/12/13 Pct Recovery = 103% Analysis Date = 01/01/13 Pct Recovery = 104% Analysis Date = 01/01/13 Pct Recovery = 104% Analysis Date = 12/22/12 Pct Recovery = 105% Analysis Date = 12/22/12 Pct Recovery = 105% Analysis Date = 12/11/12 Pct Recovery = 105% Analysis Date = 12/11/12 Pct Recovery = 105% Analysis Date = 12/01/12 Pct Recovery = 105% Analysis Date = 12/01/12 Pct Recovery = 105% Analysis Date = 11/20/12 Pct Recovery = 106% Analysis Date = 11/20/12 Pct Recovery = 106% Analysis Date = 11/10/12 Pct Recovery = 106% Analysis Date = 11/10/12 Pct Recovery = 106% Analysis Date = 10/30/12 Pct Recovery = 106% Analysis Date = 10/30/12 Pct Recovery = 106% Analysis Date = 10/19/12 Pct Recovery = 106% Analysis Date = 10/19/12 Pct Recovery = 106% Analysis Date = 10/09/12 Pct Recovery = 106% Analysis Date = 10/09/12 Pct Recovery = 106% Analysis Date = 09/28/12 Pct Recovery = 107% Analysis Date = 09/28/12 Pct Recovery = 107% Analysis Date = 09/18/12 Pct Recovery = 107% Analysis Date = 09/18/12 Pct Recovery = 107% Analysis Date = 09/07/12 Pct Recovery = 107% Analysis Date = 09/07/12 Pct Recovery = 107% Analysis Date = 08/28/12 Pct Recovery = 107% Analysis Date = 08/28/12 Pct Recovery = 107% Analysis Date = 08/17/12 Pct Recovery = 107% Analysis Date = 08/17/12 Pct Recovery = 107% Analysis Date = 08/07/12 Pct Recovery = 107% Analysis Date = 08/07/12 Pct Recovery = 107% Analysis Date = 07/27/12 Pct Recovery = 107% Analysis Date = 07/27/12 Pct Recovery = 107% Analysis Date = 07/17/12 Pct Recovery = 106% Analysis Date = 07/17/12 Pct Recovery = 106% Analysis Date = 07/06/12 Pct Recovery = 106% Analysis Date = 07/06/12 Pct Recovery = 106% Analysis Date = 06/26/12 Pct Recovery = 106% Analysis Date = 06/26/12 Pct Recovery = 106% Analysis Date = 06/15/12 Pct Recovery = 105% Analysis Date = 06/15/12 Pct Recovery = 105% Analysis Date = 06/05/12 Pct Recovery = 105% Analysis Date = 06/05/12 Pct Recovery = 105% Analysis Date = 05/25/12 Pct Recovery = 105% Analysis Date = 05/25/12 Pct Recovery = 105% Analysis Date = 05/14/12 Pct Recovery = 104% Analysis Date = 05/14/12 Pct Recovery = 104% Analysis Date = 05/04/12 Pct Recovery = 104% Analysis Date = 05/04/12 Pct Recovery = 104% Analysis Date = 04/23/12 Pct Recovery = 104% Analysis Date = 04/23/12 Pct Recovery = 104% Analysis Date = 04/13/12 Pct Recovery = 104% Analysis Date = 04/13/12 Pct Recovery = 104% Analysis Date = 04/02/12 Pct Recovery = 103% Analysis Date = 04/02/12 Pct Recovery = 103% Analysis Date = 03/23/12 Pct Recovery = 103% Analysis Date = 03/23/12 Pct Recovery = 103% Analysis Date = 03/12/12 Pct Recovery = 103% Analysis Date = 03/12/12 Pct Recovery = 103% Analysis Date = 03/02/12 Pct Recovery = 102% Analysis Date = 03/02/12 Pct Recovery = 102% Analysis Date = 02/20/12 Pct Recovery = 102% Analysis Date = 02/20/12 Pct Recovery = 102% Analysis Date = 02/10/12 Pct Recovery = 101% Analysis Date = 02/10/12 Pct Recovery = 101% Analysis Date = 01/30/12 Pct Recovery = 101% Analysis Date = 01/30/12 Pct Recovery = 101% Analysis Date = 01/20/12 Pct Recovery = 101% Analysis Date = 01/20/12 Pct Recovery = 101% Analysis Date = 01/09/12 Pct Recovery = 100% Analysis Date = 01/09/12 Pct Recovery = 100% Analysis Date = 12/29/11 Pct Recovery = 100% Analysis Date = 12/29/11 Pct Recovery = 100% Analysis Date = 12/19/11 Pct Recovery = 100% Analysis Date = 12/19/11 Pct Recovery = 100% Analysis Date = 12/08/11 Pct Recovery = 99% Analysis Date = 12/08/11 Pct Recovery = 99% Analysis Date = 11/28/11 Pct Recovery = 99% Analysis Date = 11/28/11 Pct Recovery = 99% Analysis Date = 11/17/11 Pct Recovery = 98% Analysis Date = 11/17/11 Pct Recovery = 98% Analysis Date = 11/07/11 Pct Recovery = 98% Analysis Date = 11/07/11 Pct Recovery = 98% Analysis Date = 10/27/11 Pct Recovery = 98% Analysis Date = 10/27/11 Pct Recovery = 98% Analysis Date = 10/17/11 Pct Recovery = 97% Analysis Date = 10/17/11 Pct Recovery = 97% Analysis Date = 10/06/11 Pct Recovery = 97% Analysis Date = 10/06/11 Pct Recovery = 97% Analysis Date = 09/26/11 Pct Recovery = 96% Analysis Date = 09/26/11 Pct Recovery = 96% Analysis Date = 09/15/11 Pct Recovery = 96% Analysis Date = 09/15/11 Pct Recovery = 96% Analysis Date = 09/05/11 Pct Recovery = 95% Analysis Date = 09/05/11 Pct Recovery = 95% Analysis Date = 08/25/11 Pct Recovery = 95% Analysis Date = 08/25/11 Pct Recovery = 95% Analysis Date = 08/15/11 Pct Recovery = 95% Analysis Date = 08/15/11 Pct Recovery = 95% Analysis Date = 08/04/11 Pct Recovery = 94% Analysis Date = 08/04/11 Pct Recovery = 94% Analysis Date = 07/24/11 Pct Recovery = 94% Analysis Date = 07/24/11 Pct Recovery = 94% Analysis Date = 07/14/11 Pct Recovery = 93% Analysis Date = 07/14/11 Pct Recovery = 93% Analysis Date = 07/03/11 Pct Recovery = 93% Analysis Date = 07/03/11 Pct Recovery = 93% Analysis Date = 06/23/11 Pct Recovery = 92% Analysis Date = 06/23/11 Pct Recovery = 92% Analysis Date = 06/12/11 Pct Recovery = 92% Analysis Date = 06/12/11 Pct Recovery = 92% Analysis Date = 06/02/11 Pct Recovery = 91% Analysis Date = 06/02/11 Pct Recovery = 91% Analysis Date = 05/22/11 Pct Recovery = 91% Analysis Date = 05/22/11 Pct Recovery = 91% Analysis Date = 05/12/11 Pct Recovery = 90% Analysis Date = 05/12/11 Pct Recovery = 90% Analysis Date = 05/01/11 Pct Recovery = 90% Analysis Date = 05/01/11 Pct Recovery = 90% Analysis Date = 04/21/11 Pct Recovery = 89% Analysis Date = 04/21/11 Pct Recovery = 89% Analysis Date = 04/10/11 Pct Recovery = 89% Analysis Date = 04/10/11 Pct Recovery = 89% Analysis Date = 03/31/11 Pct Recovery = 88% Analysis Date = 03/31/11 Pct Recovery = 88% Analysis Date = 03/20/11 Pct Recovery = 88% Analysis Date = 03/20/11 Pct Recovery = 88% Analysis Date = 03/10/11 Pct Recovery = 87% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
3-BETA-COPROSTANOL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 60 82% 27% 78% 28%
Total 60 82% 27% 78% 28%

Sample Statistics
3-BETA-COPROSTANOL

Characteristic N % % Basis
Plotted 60 77% Spiked
Estimated Values 3 4% Spiked
Deleted Values 3 2% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 80 .  
False Negatives 18 23% 18 out of 78
Not Spiked 51 .  
False Positives 0 0% 0 out of 50

BQS OBSP Determination:
4,4BISPHENOL F
METHOD: 4434 , TESTIDCODE: 51294GM005
Open Data Set

Analysis Date = 12/15/16 SpikeMix = Abs 061416H: 50 µl & ChemService 5016100: 50 µl Pct Recovery = 83% Analysis Date = 01/08/16 SpikeMix = Spex Organics EN150501025: 60 µl & ERA 0601-15-04: 60 µl Pct Recovery = 123% Analysis Date = 01/07/16 SpikeMix = Crescent 04EE007: 60 µl & Abs 041515: 60 µl Pct Recovery = 137% Analysis Date = 07/12/16 SpikeMix = Spex Organics EN150501025: 50 µl & ERA 0601-15-04: 50 µl Pct Recovery = 64% Analysis Date = 06/24/16 SpikeMix = Crescent 04EE007: 50 µl & Spex Organics EN150501025: 50 µl Pct Recovery = 160% Analysis Date = 01/08/16 SpikeMix = Crescent 04EE007: 50 µl & Spex Organics EN150501025: 50 µl Pct Recovery = 84% Analysis Date = 07/21/15 SpikeMix = Supelco LC13547: 50 µl & Spex Organics EN150501025: 50 µl Pct Recovery = 44% Analysis Date = 03/07/16 SpikeMix = Abs 041515: 50 µl & ERA 0601-15-04: 50 µl Pct Recovery = 117% Analysis Date = 12/10/15 SpikeMix = Abs 041515: 50 µl & ERA 0601-15-04: 50 µl Pct Recovery = 109% Analysis Date = 08/17/15 SpikeMix = ChemService 4073900: 50 µl & Abs 041515: 50 µl Pct Recovery = 88% Analysis Date = 12/05/16 SpikeMix = Abs 052616: 30 µl & Abs 061416H: 30 µl Pct Recovery = 93% Analysis Date = 03/18/16 SpikeMix = Crescent 04EE007: 30 µl & Spex Organics EN150501025: 30 µl Pct Recovery = 87% Analysis Date = 03/18/16 SpikeMix = Spex Organics EN150501025: 30 µl & Supelco LC13547: 30 µl Pct Recovery = 80% Analysis Date = 12/11/15 SpikeMix = Crescent 04EE007: 30 µl & Spex Organics EN150501025: 30 µl Pct Recovery = 80% Analysis Date = 09/23/15 SpikeMix = ChemService 4073900: 30 µl & Spex Organics EN150501025: 30 µl Pct Recovery = 127% Analysis Date = 09/17/15 SpikeMix = Supelco LC13547: 30 µl & Spex Organics EN150501025: 30 µl Pct Recovery = 87% Analysis Date = 03/07/16 SpikeMix = ChemService 4073900: 30 µl & Abs 041515: 30 µl Pct Recovery = 121% Analysis Date = 09/17/15 SpikeMix = Supelco LC13547: 30 µl & Abs 041515: 30 µl Pct Recovery = 87% Analysis Date = 06/29/15 SpikeMix = Supelco LC13547: 30 µl & Abs 041515: 30 µl Pct Recovery = 134% Analysis Date = 12/14/16 Pct Recovery = 88% Analysis Date = 12/12/16 Pct Recovery = 88% Analysis Date = 12/12/16 Pct Recovery = 88% Analysis Date = 12/09/16 Pct Recovery = 88% Analysis Date = 12/09/16 Pct Recovery = 88% Analysis Date = 12/06/16 Pct Recovery = 89% Analysis Date = 12/06/16 Pct Recovery = 89% Analysis Date = 12/04/16 Pct Recovery = 89% Analysis Date = 12/04/16 Pct Recovery = 89% Analysis Date = 12/01/16 Pct Recovery = 89% Analysis Date = 12/01/16 Pct Recovery = 89% Analysis Date = 11/28/16 Pct Recovery = 90% Analysis Date = 11/28/16 Pct Recovery = 90% Analysis Date = 11/26/16 Pct Recovery = 90% Analysis Date = 11/26/16 Pct Recovery = 90% Analysis Date = 11/23/16 Pct Recovery = 90% Analysis Date = 11/23/16 Pct Recovery = 90% Analysis Date = 11/20/16 Pct Recovery = 90% Analysis Date = 11/20/16 Pct Recovery = 90% Analysis Date = 11/18/16 Pct Recovery = 91% Analysis Date = 11/18/16 Pct Recovery = 91% Analysis Date = 11/15/16 Pct Recovery = 91% Analysis Date = 11/15/16 Pct Recovery = 91% Analysis Date = 11/12/16 Pct Recovery = 91% Analysis Date = 11/12/16 Pct Recovery = 91% Analysis Date = 11/10/16 Pct Recovery = 92% Analysis Date = 11/10/16 Pct Recovery = 92% Analysis Date = 11/07/16 Pct Recovery = 92% Analysis Date = 11/07/16 Pct Recovery = 92% Analysis Date = 11/04/16 Pct Recovery = 92% Analysis Date = 11/04/16 Pct Recovery = 92% Analysis Date = 11/02/16 Pct Recovery = 92% Analysis Date = 11/02/16 Pct Recovery = 92% Analysis Date = 10/30/16 Pct Recovery = 93% Analysis Date = 10/30/16 Pct Recovery = 93% Analysis Date = 10/27/16 Pct Recovery = 93% Analysis Date = 10/27/16 Pct Recovery = 93% Analysis Date = 10/25/16 Pct Recovery = 93% Analysis Date = 10/25/16 Pct Recovery = 93% Analysis Date = 10/22/16 Pct Recovery = 93% Analysis Date = 10/22/16 Pct Recovery = 93% Analysis Date = 10/19/16 Pct Recovery = 94% Analysis Date = 10/19/16 Pct Recovery = 94% Analysis Date = 10/17/16 Pct Recovery = 94% Analysis Date = 10/17/16 Pct Recovery = 94% Analysis Date = 10/14/16 Pct Recovery = 94% Analysis Date = 10/14/16 Pct Recovery = 94% Analysis Date = 10/11/16 Pct Recovery = 95% Analysis Date = 10/11/16 Pct Recovery = 95% Analysis Date = 10/09/16 Pct Recovery = 95% Analysis Date = 10/09/16 Pct Recovery = 95% Analysis Date = 10/06/16 Pct Recovery = 95% Analysis Date = 10/06/16 Pct Recovery = 95% Analysis Date = 10/03/16 Pct Recovery = 95% Analysis Date = 10/03/16 Pct Recovery = 95% Analysis Date = 10/01/16 Pct Recovery = 96% Analysis Date = 10/01/16 Pct Recovery = 96% Analysis Date = 09/28/16 Pct Recovery = 96% Analysis Date = 09/28/16 Pct Recovery = 96% Analysis Date = 09/25/16 Pct Recovery = 96% Analysis Date = 09/25/16 Pct Recovery = 96% Analysis Date = 09/23/16 Pct Recovery = 97% Analysis Date = 09/23/16 Pct Recovery = 97% Analysis Date = 09/20/16 Pct Recovery = 97% Analysis Date = 09/20/16 Pct Recovery = 97% Analysis Date = 09/17/16 Pct Recovery = 97% Analysis Date = 09/17/16 Pct Recovery = 97% Analysis Date = 09/15/16 Pct Recovery = 97% Analysis Date = 09/15/16 Pct Recovery = 97% Analysis Date = 09/12/16 Pct Recovery = 98% Analysis Date = 09/12/16 Pct Recovery = 98% Analysis Date = 09/09/16 Pct Recovery = 98% Analysis Date = 09/09/16 Pct Recovery = 98% Analysis Date = 09/07/16 Pct Recovery = 98% Analysis Date = 09/07/16 Pct Recovery = 98% Analysis Date = 09/04/16 Pct Recovery = 99% Analysis Date = 09/04/16 Pct Recovery = 99% Analysis Date = 09/01/16 Pct Recovery = 99% Analysis Date = 09/01/16 Pct Recovery = 99% Analysis Date = 08/29/16 Pct Recovery = 99% Analysis Date = 08/29/16 Pct Recovery = 99% Analysis Date = 08/27/16 Pct Recovery = 99% Analysis Date = 08/27/16 Pct Recovery = 99% Analysis Date = 08/24/16 Pct Recovery = 100% Analysis Date = 08/24/16 Pct Recovery = 100% Analysis Date = 08/21/16 Pct Recovery = 100% Analysis Date = 08/21/16 Pct Recovery = 100% Analysis Date = 08/19/16 Pct Recovery = 100% Analysis Date = 08/19/16 Pct Recovery = 100% Analysis Date = 08/16/16 Pct Recovery = 100% Analysis Date = 08/16/16 Pct Recovery = 100% Analysis Date = 08/13/16 Pct Recovery = 101% Analysis Date = 08/13/16 Pct Recovery = 101% Analysis Date = 08/11/16 Pct Recovery = 101% Analysis Date = 08/11/16 Pct Recovery = 101% Analysis Date = 08/08/16 Pct Recovery = 101% Analysis Date = 08/08/16 Pct Recovery = 101% Analysis Date = 08/05/16 Pct Recovery = 102% Analysis Date = 08/05/16 Pct Recovery = 102% Analysis Date = 08/03/16 Pct Recovery = 102% Analysis Date = 08/03/16 Pct Recovery = 102% Analysis Date = 07/31/16 Pct Recovery = 102% Analysis Date = 07/31/16 Pct Recovery = 102% Analysis Date = 07/28/16 Pct Recovery = 102% Analysis Date = 07/28/16 Pct Recovery = 102% Analysis Date = 07/26/16 Pct Recovery = 103% Analysis Date = 07/26/16 Pct Recovery = 103% Analysis Date = 07/23/16 Pct Recovery = 103% Analysis Date = 07/23/16 Pct Recovery = 103% Analysis Date = 07/20/16 Pct Recovery = 103% Analysis Date = 07/20/16 Pct Recovery = 103% Analysis Date = 07/18/16 Pct Recovery = 104% Analysis Date = 07/18/16 Pct Recovery = 104% Analysis Date = 07/15/16 Pct Recovery = 104% Analysis Date = 07/15/16 Pct Recovery = 104% Analysis Date = 07/12/16 Pct Recovery = 104% Analysis Date = 07/12/16 Pct Recovery = 104% Analysis Date = 07/10/16 Pct Recovery = 104% Analysis Date = 07/10/16 Pct Recovery = 104% Analysis Date = 07/07/16 Pct Recovery = 104% Analysis Date = 07/07/16 Pct Recovery = 104% Analysis Date = 07/04/16 Pct Recovery = 104% Analysis Date = 07/04/16 Pct Recovery = 104% Analysis Date = 07/02/16 Pct Recovery = 104% Analysis Date = 07/02/16 Pct Recovery = 104% Analysis Date = 06/29/16 Pct Recovery = 104% Analysis Date = 06/29/16 Pct Recovery = 104% Analysis Date = 06/26/16 Pct Recovery = 104% Analysis Date = 06/26/16 Pct Recovery = 104% Analysis Date = 06/24/16 Pct Recovery = 104% Analysis Date = 06/24/16 Pct Recovery = 104% Analysis Date = 06/21/16 Pct Recovery = 104% Analysis Date = 06/21/16 Pct Recovery = 104% Analysis Date = 06/18/16 Pct Recovery = 104% Analysis Date = 06/18/16 Pct Recovery = 104% Analysis Date = 06/16/16 Pct Recovery = 104% Analysis Date = 06/16/16 Pct Recovery = 104% Analysis Date = 06/13/16 Pct Recovery = 104% Analysis Date = 06/13/16 Pct Recovery = 104% Analysis Date = 06/10/16 Pct Recovery = 104% Analysis Date = 06/10/16 Pct Recovery = 104% Analysis Date = 06/08/16 Pct Recovery = 104% Analysis Date = 06/08/16 Pct Recovery = 104% Analysis Date = 06/05/16 Pct Recovery = 103% Analysis Date = 06/05/16 Pct Recovery = 103% Analysis Date = 06/02/16 Pct Recovery = 103% Analysis Date = 06/02/16 Pct Recovery = 103% Analysis Date = 05/31/16 Pct Recovery = 103% Analysis Date = 05/31/16 Pct Recovery = 103% Analysis Date = 05/28/16 Pct Recovery = 103% Analysis Date = 05/28/16 Pct Recovery = 103% Analysis Date = 05/25/16 Pct Recovery = 103% Analysis Date = 05/25/16 Pct Recovery = 103% Analysis Date = 05/23/16 Pct Recovery = 103% Analysis Date = 05/23/16 Pct Recovery = 103% Analysis Date = 05/20/16 Pct Recovery = 103% Analysis Date = 05/20/16 Pct Recovery = 103% Analysis Date = 05/17/16 Pct Recovery = 103% Analysis Date = 05/17/16 Pct Recovery = 103% Analysis Date = 05/14/16 Pct Recovery = 103% Analysis Date = 05/14/16 Pct Recovery = 103% Analysis Date = 05/12/16 Pct Recovery = 103% Analysis Date = 05/12/16 Pct Recovery = 103% Analysis Date = 05/09/16 Pct Recovery = 103% Analysis Date = 05/09/16 Pct Recovery = 103% Analysis Date = 05/06/16 Pct Recovery = 103% Analysis Date = 05/06/16 Pct Recovery = 103% Analysis Date = 05/04/16 Pct Recovery = 103% Analysis Date = 05/04/16 Pct Recovery = 103% Analysis Date = 05/01/16 Pct Recovery = 103% Analysis Date = 05/01/16 Pct Recovery = 103% Analysis Date = 04/28/16 Pct Recovery = 103% Analysis Date = 04/28/16 Pct Recovery = 103% Analysis Date = 04/26/16 Pct Recovery = 103% Analysis Date = 04/26/16 Pct Recovery = 103% Analysis Date = 04/23/16 Pct Recovery = 103% Analysis Date = 04/23/16 Pct Recovery = 103% Analysis Date = 04/20/16 Pct Recovery = 103% Analysis Date = 04/20/16 Pct Recovery = 103% Analysis Date = 04/18/16 Pct Recovery = 103% Analysis Date = 04/18/16 Pct Recovery = 103% Analysis Date = 04/15/16 Pct Recovery = 102% Analysis Date = 04/15/16 Pct Recovery = 102% Analysis Date = 04/12/16 Pct Recovery = 102% Analysis Date = 04/12/16 Pct Recovery = 102% Analysis Date = 04/10/16 Pct Recovery = 102% Analysis Date = 04/10/16 Pct Recovery = 102% Analysis Date = 04/07/16 Pct Recovery = 102% Analysis Date = 04/07/16 Pct Recovery = 102% Analysis Date = 04/04/16 Pct Recovery = 102% Analysis Date = 04/04/16 Pct Recovery = 102% Analysis Date = 04/02/16 Pct Recovery = 102% Analysis Date = 04/02/16 Pct Recovery = 102% Analysis Date = 03/30/16 Pct Recovery = 102% Analysis Date = 03/30/16 Pct Recovery = 102% Analysis Date = 03/27/16 Pct Recovery = 102% Analysis Date = 03/27/16 Pct Recovery = 102% Analysis Date = 03/25/16 Pct Recovery = 102% Analysis Date = 03/25/16 Pct Recovery = 102% Analysis Date = 03/22/16 Pct Recovery = 102% Analysis Date = 03/22/16 Pct Recovery = 102% Analysis Date = 03/19/16 Pct Recovery = 102% Analysis Date = 03/19/16 Pct Recovery = 102% Analysis Date = 03/17/16 Pct Recovery = 102% Analysis Date = 03/17/16 Pct Recovery = 102% Analysis Date = 03/14/16 Pct Recovery = 102% Analysis Date = 03/14/16 Pct Recovery = 102% Analysis Date = 03/11/16 Pct Recovery = 103% Analysis Date = 03/11/16 Pct Recovery = 103% Analysis Date = 03/09/16 Pct Recovery = 103% Analysis Date = 03/09/16 Pct Recovery = 103% Analysis Date = 03/06/16 Pct Recovery = 103% Analysis Date = 03/06/16 Pct Recovery = 103% Analysis Date = 03/03/16 Pct Recovery = 103% Analysis Date = 03/03/16 Pct Recovery = 103% Analysis Date = 03/01/16 Pct Recovery = 103% Analysis Date = 03/01/16 Pct Recovery = 103% Analysis Date = 02/27/16 Pct Recovery = 104% Analysis Date = 02/27/16 Pct Recovery = 104% Analysis Date = 02/24/16 Pct Recovery = 104% Analysis Date = 02/24/16 Pct Recovery = 104% Analysis Date = 02/22/16 Pct Recovery = 104% Analysis Date = 02/22/16 Pct Recovery = 104% Analysis Date = 02/19/16 Pct Recovery = 104% Analysis Date = 02/19/16 Pct Recovery = 104% Analysis Date = 02/16/16 Pct Recovery = 104% Analysis Date = 02/16/16 Pct Recovery = 104% Analysis Date = 02/14/16 Pct Recovery = 104% Analysis Date = 02/14/16 Pct Recovery = 104% Analysis Date = 02/11/16 Pct Recovery = 104% Analysis Date = 02/11/16 Pct Recovery = 104% Analysis Date = 02/08/16 Pct Recovery = 104% Analysis Date = 02/08/16 Pct Recovery = 104% Analysis Date = 02/06/16 Pct Recovery = 105% Analysis Date = 02/06/16 Pct Recovery = 105% Analysis Date = 02/03/16 Pct Recovery = 105% Analysis Date = 02/03/16 Pct Recovery = 105% Analysis Date = 01/31/16 Pct Recovery = 105% Analysis Date = 01/31/16 Pct Recovery = 105% Analysis Date = 01/28/16 Pct Recovery = 105% Analysis Date = 01/28/16 Pct Recovery = 105% Analysis Date = 01/26/16 Pct Recovery = 105% Analysis Date = 01/26/16 Pct Recovery = 105% Analysis Date = 01/23/16 Pct Recovery = 105% Analysis Date = 01/23/16 Pct Recovery = 105% Analysis Date = 01/20/16 Pct Recovery = 105% Analysis Date = 01/20/16 Pct Recovery = 105% Analysis Date = 01/18/16 Pct Recovery = 105% Analysis Date = 01/18/16 Pct Recovery = 105% Analysis Date = 01/15/16 Pct Recovery = 106% Analysis Date = 01/15/16 Pct Recovery = 106% Analysis Date = 01/12/16 Pct Recovery = 106% Analysis Date = 01/12/16 Pct Recovery = 106% Analysis Date = 01/10/16 Pct Recovery = 106% Analysis Date = 01/10/16 Pct Recovery = 106% Analysis Date = 01/07/16 Pct Recovery = 106% Analysis Date = 01/07/16 Pct Recovery = 106% Analysis Date = 01/04/16 Pct Recovery = 106% Analysis Date = 01/04/16 Pct Recovery = 106% Analysis Date = 01/02/16 Pct Recovery = 105% Analysis Date = 01/02/16 Pct Recovery = 105% Analysis Date = 12/30/15 Pct Recovery = 105% Analysis Date = 12/30/15 Pct Recovery = 105% Analysis Date = 12/27/15 Pct Recovery = 105% Analysis Date = 12/27/15 Pct Recovery = 105% Analysis Date = 12/25/15 Pct Recovery = 105% Analysis Date = 12/25/15 Pct Recovery = 105% Analysis Date = 12/22/15 Pct Recovery = 105% Analysis Date = 12/22/15 Pct Recovery = 105% Analysis Date = 12/19/15 Pct Recovery = 104% Analysis Date = 12/19/15 Pct Recovery = 104% Analysis Date = 12/17/15 Pct Recovery = 104% Analysis Date = 12/17/15 Pct Recovery = 104% Analysis Date = 12/14/15 Pct Recovery = 104% Analysis Date = 12/14/15 Pct Recovery = 104% Analysis Date = 12/11/15 Pct Recovery = 104% Analysis Date = 12/11/15 Pct Recovery = 104% Analysis Date = 12/09/15 Pct Recovery = 104% Analysis Date = 12/09/15 Pct Recovery = 104% Analysis Date = 12/06/15 Pct Recovery = 104% Analysis Date = 12/06/15 Pct Recovery = 104% Analysis Date = 12/03/15 Pct Recovery = 103% Analysis Date = 12/03/15 Pct Recovery = 103% Analysis Date = 12/01/15 Pct Recovery = 103% Analysis Date = 12/01/15 Pct Recovery = 103% Analysis Date = 11/28/15 Pct Recovery = 103% Analysis Date = 11/28/15 Pct Recovery = 103% Analysis Date = 11/25/15 Pct Recovery = 102% Analysis Date = 11/25/15 Pct Recovery = 102% Analysis Date = 11/23/15 Pct Recovery = 102% Analysis Date = 11/23/15 Pct Recovery = 102% Analysis Date = 11/20/15 Pct Recovery = 102% Analysis Date = 11/20/15 Pct Recovery = 102% Analysis Date = 11/17/15 Pct Recovery = 101% Analysis Date = 11/17/15 Pct Recovery = 101% Analysis Date = 11/15/15 Pct Recovery = 101% Analysis Date = 11/15/15 Pct Recovery = 101% Analysis Date = 11/12/15 Pct Recovery = 101% Analysis Date = 11/12/15 Pct Recovery = 101% Analysis Date = 11/09/15 Pct Recovery = 101% Analysis Date = 11/09/15 Pct Recovery = 101% Analysis Date = 11/07/15 Pct Recovery = 100% Analysis Date = 11/07/15 Pct Recovery = 100% Analysis Date = 11/04/15 Pct Recovery = 100% Analysis Date = 11/04/15 Pct Recovery = 100% Analysis Date = 11/01/15 Pct Recovery = 100% Analysis Date = 11/01/15 Pct Recovery = 100% Analysis Date = 10/30/15 Pct Recovery = 99% Analysis Date = 10/30/15 Pct Recovery = 99% Analysis Date = 10/27/15 Pct Recovery = 99% Analysis Date = 10/27/15 Pct Recovery = 99% Analysis Date = 10/24/15 Pct Recovery = 99% Analysis Date = 10/24/15 Pct Recovery = 99% Analysis Date = 10/22/15 Pct Recovery = 98% Analysis Date = 10/22/15 Pct Recovery = 98% Analysis Date = 10/19/15 Pct Recovery = 98% Analysis Date = 10/19/15 Pct Recovery = 98% Analysis Date = 10/16/15 Pct Recovery = 98% Analysis Date = 10/16/15 Pct Recovery = 98% Analysis Date = 10/13/15 Pct Recovery = 97% Analysis Date = 10/13/15 Pct Recovery = 97% Analysis Date = 10/11/15 Pct Recovery = 97% Analysis Date = 10/11/15 Pct Recovery = 97% Analysis Date = 10/08/15 Pct Recovery = 97% Analysis Date = 10/08/15 Pct Recovery = 97% Analysis Date = 10/05/15 Pct Recovery = 96% Analysis Date = 10/05/15 Pct Recovery = 96% Analysis Date = 10/03/15 Pct Recovery = 96% Analysis Date = 10/03/15 Pct Recovery = 96% Analysis Date = 09/30/15 Pct Recovery = 96% Analysis Date = 09/30/15 Pct Recovery = 96% Analysis Date = 09/27/15 Pct Recovery = 95% Analysis Date = 09/27/15 Pct Recovery = 95% Analysis Date = 09/25/15 Pct Recovery = 95% Analysis Date = 09/25/15 Pct Recovery = 95% Analysis Date = 09/22/15 Pct Recovery = 95% Analysis Date = 09/22/15 Pct Recovery = 95% Analysis Date = 09/19/15 Pct Recovery = 95% Analysis Date = 09/19/15 Pct Recovery = 95% Analysis Date = 09/17/15 Pct Recovery = 94% Analysis Date = 09/17/15 Pct Recovery = 94% Analysis Date = 09/14/15 Pct Recovery = 94% Analysis Date = 09/14/15 Pct Recovery = 94% Analysis Date = 09/11/15 Pct Recovery = 94% Analysis Date = 09/11/15 Pct Recovery = 94% Analysis Date = 09/09/15 Pct Recovery = 94% Analysis Date = 09/09/15 Pct Recovery = 94% Analysis Date = 09/06/15 Pct Recovery = 94% Analysis Date = 09/06/15 Pct Recovery = 94% Analysis Date = 09/03/15 Pct Recovery = 94% Analysis Date = 09/03/15 Pct Recovery = 94% Analysis Date = 09/01/15 Pct Recovery = 94% Analysis Date = 09/01/15 Pct Recovery = 94% Analysis Date = 08/29/15 Pct Recovery = 94% Analysis Date = 08/29/15 Pct Recovery = 94% Analysis Date = 08/26/15 Pct Recovery = 94% Analysis Date = 08/26/15 Pct Recovery = 94% Analysis Date = 08/24/15 Pct Recovery = 94% Analysis Date = 08/24/15 Pct Recovery = 94% Analysis Date = 08/21/15 Pct Recovery = 94% Analysis Date = 08/21/15 Pct Recovery = 94% Analysis Date = 08/18/15 Pct Recovery = 93% Analysis Date = 08/18/15 Pct Recovery = 93% Analysis Date = 08/16/15 Pct Recovery = 93% Analysis Date = 08/16/15 Pct Recovery = 93% Analysis Date = 08/13/15 Pct Recovery = 93% Analysis Date = 08/13/15 Pct Recovery = 93% Analysis Date = 08/10/15 Pct Recovery = 93% Analysis Date = 08/10/15 Pct Recovery = 93% Analysis Date = 08/08/15 Pct Recovery = 94% Analysis Date = 08/08/15 Pct Recovery = 94% Analysis Date = 08/05/15 Pct Recovery = 94% Analysis Date = 08/05/15 Pct Recovery = 94% Analysis Date = 08/02/15 Pct Recovery = 94% Analysis Date = 08/02/15 Pct Recovery = 94% Analysis Date = 07/31/15 Pct Recovery = 94% Analysis Date = 07/31/15 Pct Recovery = 94% Analysis Date = 07/28/15 Pct Recovery = 94% Analysis Date = 07/28/15 Pct Recovery = 94% Analysis Date = 07/25/15 Pct Recovery = 94% Analysis Date = 07/25/15 Pct Recovery = 94% Analysis Date = 07/23/15 Pct Recovery = 94% Analysis Date = 07/23/15 Pct Recovery = 94% Analysis Date = 07/20/15 Pct Recovery = 94% Analysis Date = 07/20/15 Pct Recovery = 94% Analysis Date = 07/17/15 Pct Recovery = 94% Analysis Date = 07/17/15 Pct Recovery = 94% Analysis Date = 07/15/15 Pct Recovery = 94% Analysis Date = 07/15/15 Pct Recovery = 94% Analysis Date = 07/12/15 Pct Recovery = 94% Analysis Date = 07/12/15 Pct Recovery = 94% Analysis Date = 07/09/15 Pct Recovery = 94% Analysis Date = 07/09/15 Pct Recovery = 94% Analysis Date = 07/07/15 Pct Recovery = 94% Analysis Date = 07/07/15 Pct Recovery = 94% Analysis Date = 07/04/15 Pct Recovery = 94% Analysis Date = 07/04/15 Pct Recovery = 94% Analysis Date = 07/01/15 Pct Recovery = 94% Analysis Date = 07/01/15 Pct Recovery = 94% Analysis Date = 06/29/15 Pct Recovery = 94% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
4,4BISPHENOL F

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 19 100% 29% 88% 30%
Total 19 100% 29% 88% 30%

Sample Statistics
4,4BISPHENOL F

Characteristic N % % Basis
Plotted 19 100% Spiked
Estimated Values 19 100% Spiked
Deleted Values 1 2% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 20 .  
False Negatives 0 0% 0 out of 19
Not Spiked 27 .  
False Positives 0 0% 0 out of 27

BQS OBSP Determination:
4,4BISPHENOL S
METHOD: 4434 , TESTIDCODE: 51295GM005
Open Data Set

The SGPlot Procedure

Sample Statistics
4,4BISPHENOL S

Characteristic N % % Basis
Plotted 0 . Spiked
Estimated Values 0 . Spiked
Deleted Values 2 100% Spiked + Not Spiked
Spiked, Censored 0 . Spiked
Spiked 0 .  
False Negatives 0 . 0 out of 0
Not Spiked 2 .  
False Positives 0 . 0 out of 0

BQS OBSP Determination:
4-ANDROSTENE-3,17-DIONE
METHOD: 4434 , TESTIDCODE: 64533GM005
Open Data Set

Analysis Date = 04/22/13 SpikeMix = ERA 0507-12-04.1: 50 µl & Restek A089631: 50 µl Pct Recovery = 80% Analysis Date = 12/18/12 SpikeMix = ERA 0507-12-04.1: 50 µl & Restek A089631: 50 µl Pct Recovery = 83% Analysis Date = 11/07/12 SpikeMix = ERA 0507-12-04.1: 50 µl & ERA 0511-12-02: 50 µl Pct Recovery = 89% Analysis Date = 04/03/13 SpikeMix = Spex Organics T1120525010: 50 µl & Restek A089631: 50 µl Pct Recovery = 66% Analysis Date = 12/18/12 SpikeMix = Spex Organics T1120525010: 50 µl & Supelco LB92781: 50 µl Pct Recovery = 72% Analysis Date = 03/27/12 SpikeMix = Crescent 162776: 100 µl Pct Recovery = 118% Analysis Date = 03/10/11 SpikeMix = Crescent 162776: 100 µl Pct Recovery = 69% Analysis Date = 06/23/11 SpikeMix = Crescent 162776: 100 µl Pct Recovery = 80% Analysis Date = 02/08/13 SpikeMix = ERA 0507-12-04.1: 25 µl & Supelco LB92781: 25 µl Pct Recovery = 77% Analysis Date = 11/01/12 SpikeMix = ERA 0507-12-04.1: 25 µl & Abs 051512: 25 µl Pct Recovery = 75% Analysis Date = 04/03/13 SpikeMix = Spex Organics T1120525010: 25 µl & Abs 051512: 25 µl Pct Recovery = 64% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120525010: 25 µl & ERA 0511-12-02: 25 µl Pct Recovery = 52% Analysis Date = 08/29/12 SpikeMix = Spex Organics T1120525010: 25 µl Pct Recovery = 100% Analysis Date = 03/14/14 SpikeMix = Supelco LB99393: 50 µl & Abs 050813: 50 µl Pct Recovery = 81% Analysis Date = 03/14/14 SpikeMix = Supelco LB99393: 50 µl & Abs 060413: 50 µl & Abs 071513: 50 µl Pct Recovery = 62% Analysis Date = 03/05/14 SpikeMix = ERA 0415-13-01.1A: 50 µl & Abs 060413: 50 µl & Abs 071513: 50 µl Pct Recovery = 57% Analysis Date = 02/25/14 SpikeMix = ERA 0415-13-01.1A: 50 µl & Abs 050813: 50 µl Pct Recovery = 40% Analysis Date = 03/14/14 SpikeMix = ERA 0415-13-01.2A: 50 µl & Spex Organics T1130423008: 50 µl Pct Recovery = 45% Analysis Date = 03/05/14 SpikeMix = Spex Organics T1130423008: 50 µl & Abs 071513: 50 µl Pct Recovery = 70% Analysis Date = 08/09/13 SpikeMix = ERA 0415-13-01.2A: 50 µl & Spex Organics T1130423008: 50 µl Pct Recovery = 49% Analysis Date = 04/06/12 SpikeMix = Crescent 162776: 25 µl Pct Recovery = 92% Analysis Date = 11/17/11 SpikeMix = Crescent 162776: 25 µl Pct Recovery = 75% Analysis Date = 10/12/11 SpikeMix = Crescent 162776: 25 µl Pct Recovery = 86% Analysis Date = 07/25/11 SpikeMix = Crescent 162776: 25 µl Pct Recovery = 70% Analysis Date = 05/09/11 SpikeMix = Crescent 162776: 25 µl Pct Recovery = 82% Analysis Date = 04/14/14 SpikeMix = ERA 0415-13-01.1A: 20 µl & ERA 0415-13-01.2A: 20 µl & Abs 060413: 20 µl Pct Recovery = 46% Analysis Date = 03/03/14 SpikeMix = Abs 050813: 20 µl & Abs 071513: 20 µl Pct Recovery = 35% Analysis Date = 02/19/14 SpikeMix = Abs 050813: 20 µl & Abs 071513: 20 µl Pct Recovery = 78% Analysis Date = 01/23/14 SpikeMix = Supelco LB99393: 20 µl & ERA 0415-13-01.2A: 20 µl & Abs 060413: 20 µl Pct Recovery = 68% Analysis Date = 11/18/13 SpikeMix = ERA 0415-13-01.2A: 20 µl & Abs 050813: 20 µl Pct Recovery = 68% Analysis Date = 09/16/13 SpikeMix = ERA 0415-13-01.1A: 20 µl & ERA 0415-13-01.2A: 20 µl & Abs 060413: 20 µl Pct Recovery = 55% Analysis Date = 12/09/13 SpikeMix = Supelco LB99393: 20 µl & Spex Organics T1130423008: 20 µl Pct Recovery = 55% Analysis Date = 06/27/13 SpikeMix = ERA 0415-13-01.1A: 20 µl & Spex Organics T1130423008: 20 µl Pct Recovery = 38% Analysis Date = 06/04/13 SpikeMix = Supelco LB99393: 20 µl & Spex Organics T1130423008: 20 µl Pct Recovery = 33% Analysis Date = 08/10/15 SpikeMix = ERA 0601-15-04: 50 µl & Crescent 04EE007: 50 µl Pct Recovery = 89% Analysis Date = 08/09/15 Pct Recovery = 87% Analysis Date = 08/01/15 Pct Recovery = 87% Analysis Date = 08/01/15 Pct Recovery = 87% Analysis Date = 07/24/15 Pct Recovery = 86% Analysis Date = 07/24/15 Pct Recovery = 86% Analysis Date = 07/16/15 Pct Recovery = 86% Analysis Date = 07/16/15 Pct Recovery = 86% Analysis Date = 07/08/15 Pct Recovery = 85% Analysis Date = 07/08/15 Pct Recovery = 85% Analysis Date = 06/30/15 Pct Recovery = 85% Analysis Date = 06/30/15 Pct Recovery = 85% Analysis Date = 06/22/15 Pct Recovery = 84% Analysis Date = 06/22/15 Pct Recovery = 84% Analysis Date = 06/14/15 Pct Recovery = 84% Analysis Date = 06/14/15 Pct Recovery = 84% Analysis Date = 06/06/15 Pct Recovery = 83% Analysis Date = 06/06/15 Pct Recovery = 83% Analysis Date = 05/29/15 Pct Recovery = 83% Analysis Date = 05/29/15 Pct Recovery = 83% Analysis Date = 05/21/15 Pct Recovery = 82% Analysis Date = 05/21/15 Pct Recovery = 82% Analysis Date = 05/13/15 Pct Recovery = 82% Analysis Date = 05/13/15 Pct Recovery = 82% Analysis Date = 05/05/15 Pct Recovery = 82% Analysis Date = 05/05/15 Pct Recovery = 82% Analysis Date = 04/27/15 Pct Recovery = 81% Analysis Date = 04/27/15 Pct Recovery = 81% Analysis Date = 04/19/15 Pct Recovery = 81% Analysis Date = 04/19/15 Pct Recovery = 81% Analysis Date = 04/10/15 Pct Recovery = 80% Analysis Date = 04/10/15 Pct Recovery = 80% Analysis Date = 04/02/15 Pct Recovery = 80% Analysis Date = 04/02/15 Pct Recovery = 80% Analysis Date = 03/25/15 Pct Recovery = 79% Analysis Date = 03/25/15 Pct Recovery = 79% Analysis Date = 03/17/15 Pct Recovery = 79% Analysis Date = 03/17/15 Pct Recovery = 79% Analysis Date = 03/09/15 Pct Recovery = 78% Analysis Date = 03/09/15 Pct Recovery = 78% Analysis Date = 03/01/15 Pct Recovery = 78% Analysis Date = 03/01/15 Pct Recovery = 78% Analysis Date = 02/21/15 Pct Recovery = 78% Analysis Date = 02/21/15 Pct Recovery = 78% Analysis Date = 02/13/15 Pct Recovery = 77% Analysis Date = 02/13/15 Pct Recovery = 77% Analysis Date = 02/05/15 Pct Recovery = 77% Analysis Date = 02/05/15 Pct Recovery = 77% Analysis Date = 01/28/15 Pct Recovery = 76% Analysis Date = 01/28/15 Pct Recovery = 76% Analysis Date = 01/20/15 Pct Recovery = 76% Analysis Date = 01/20/15 Pct Recovery = 76% Analysis Date = 01/12/15 Pct Recovery = 75% Analysis Date = 01/12/15 Pct Recovery = 75% Analysis Date = 01/04/15 Pct Recovery = 75% Analysis Date = 01/04/15 Pct Recovery = 75% Analysis Date = 12/27/14 Pct Recovery = 74% Analysis Date = 12/27/14 Pct Recovery = 74% Analysis Date = 12/18/14 Pct Recovery = 74% Analysis Date = 12/18/14 Pct Recovery = 74% Analysis Date = 12/10/14 Pct Recovery = 74% Analysis Date = 12/10/14 Pct Recovery = 74% Analysis Date = 12/02/14 Pct Recovery = 73% Analysis Date = 12/02/14 Pct Recovery = 73% Analysis Date = 11/24/14 Pct Recovery = 73% Analysis Date = 11/24/14 Pct Recovery = 73% Analysis Date = 11/16/14 Pct Recovery = 72% Analysis Date = 11/16/14 Pct Recovery = 72% Analysis Date = 11/08/14 Pct Recovery = 72% Analysis Date = 11/08/14 Pct Recovery = 72% Analysis Date = 10/31/14 Pct Recovery = 71% Analysis Date = 10/31/14 Pct Recovery = 71% Analysis Date = 10/23/14 Pct Recovery = 71% Analysis Date = 10/23/14 Pct Recovery = 71% Analysis Date = 10/15/14 Pct Recovery = 70% Analysis Date = 10/15/14 Pct Recovery = 70% Analysis Date = 10/07/14 Pct Recovery = 70% Analysis Date = 10/07/14 Pct Recovery = 70% Analysis Date = 09/29/14 Pct Recovery = 69% Analysis Date = 09/29/14 Pct Recovery = 69% Analysis Date = 09/21/14 Pct Recovery = 69% Analysis Date = 09/21/14 Pct Recovery = 69% Analysis Date = 09/13/14 Pct Recovery = 69% Analysis Date = 09/13/14 Pct Recovery = 69% Analysis Date = 09/05/14 Pct Recovery = 68% Analysis Date = 09/05/14 Pct Recovery = 68% Analysis Date = 08/27/14 Pct Recovery = 68% Analysis Date = 08/27/14 Pct Recovery = 68% Analysis Date = 08/19/14 Pct Recovery = 67% Analysis Date = 08/19/14 Pct Recovery = 67% Analysis Date = 08/11/14 Pct Recovery = 67% Analysis Date = 08/11/14 Pct Recovery = 67% Analysis Date = 08/03/14 Pct Recovery = 66% Analysis Date = 08/03/14 Pct Recovery = 66% Analysis Date = 07/26/14 Pct Recovery = 66% Analysis Date = 07/26/14 Pct Recovery = 66% Analysis Date = 07/18/14 Pct Recovery = 65% Analysis Date = 07/18/14 Pct Recovery = 65% Analysis Date = 07/10/14 Pct Recovery = 65% Analysis Date = 07/10/14 Pct Recovery = 65% Analysis Date = 07/02/14 Pct Recovery = 65% Analysis Date = 07/02/14 Pct Recovery = 65% Analysis Date = 06/24/14 Pct Recovery = 64% Analysis Date = 06/24/14 Pct Recovery = 64% Analysis Date = 06/16/14 Pct Recovery = 64% Analysis Date = 06/16/14 Pct Recovery = 64% Analysis Date = 06/08/14 Pct Recovery = 63% Analysis Date = 06/08/14 Pct Recovery = 63% Analysis Date = 05/31/14 Pct Recovery = 63% Analysis Date = 05/31/14 Pct Recovery = 63% Analysis Date = 05/23/14 Pct Recovery = 62% Analysis Date = 05/23/14 Pct Recovery = 62% Analysis Date = 05/15/14 Pct Recovery = 62% Analysis Date = 05/15/14 Pct Recovery = 62% Analysis Date = 05/07/14 Pct Recovery = 61% Analysis Date = 05/07/14 Pct Recovery = 61% Analysis Date = 04/28/14 Pct Recovery = 61% Analysis Date = 04/28/14 Pct Recovery = 61% Analysis Date = 04/20/14 Pct Recovery = 61% Analysis Date = 04/20/14 Pct Recovery = 61% Analysis Date = 04/12/14 Pct Recovery = 60% Analysis Date = 04/12/14 Pct Recovery = 60% Analysis Date = 04/04/14 Pct Recovery = 60% Analysis Date = 04/04/14 Pct Recovery = 60% Analysis Date = 03/27/14 Pct Recovery = 59% Analysis Date = 03/27/14 Pct Recovery = 59% Analysis Date = 03/19/14 Pct Recovery = 59% Analysis Date = 03/19/14 Pct Recovery = 59% Analysis Date = 03/11/14 Pct Recovery = 58% Analysis Date = 03/11/14 Pct Recovery = 58% Analysis Date = 03/03/14 Pct Recovery = 58% Analysis Date = 03/03/14 Pct Recovery = 58% Analysis Date = 02/23/14 Pct Recovery = 58% Analysis Date = 02/23/14 Pct Recovery = 58% Analysis Date = 02/15/14 Pct Recovery = 58% Analysis Date = 02/15/14 Pct Recovery = 58% Analysis Date = 02/07/14 Pct Recovery = 58% Analysis Date = 02/07/14 Pct Recovery = 58% Analysis Date = 01/30/14 Pct Recovery = 57% Analysis Date = 01/30/14 Pct Recovery = 57% Analysis Date = 01/22/14 Pct Recovery = 57% Analysis Date = 01/22/14 Pct Recovery = 57% Analysis Date = 01/14/14 Pct Recovery = 57% Analysis Date = 01/14/14 Pct Recovery = 57% Analysis Date = 01/05/14 Pct Recovery = 57% Analysis Date = 01/05/14 Pct Recovery = 57% Analysis Date = 12/28/13 Pct Recovery = 57% Analysis Date = 12/28/13 Pct Recovery = 57% Analysis Date = 12/20/13 Pct Recovery = 56% Analysis Date = 12/20/13 Pct Recovery = 56% Analysis Date = 12/12/13 Pct Recovery = 56% Analysis Date = 12/12/13 Pct Recovery = 56% Analysis Date = 12/04/13 Pct Recovery = 56% Analysis Date = 12/04/13 Pct Recovery = 56% Analysis Date = 11/26/13 Pct Recovery = 56% Analysis Date = 11/26/13 Pct Recovery = 56% Analysis Date = 11/18/13 Pct Recovery = 56% Analysis Date = 11/18/13 Pct Recovery = 56% Analysis Date = 11/10/13 Pct Recovery = 56% Analysis Date = 11/10/13 Pct Recovery = 56% Analysis Date = 11/02/13 Pct Recovery = 56% Analysis Date = 11/02/13 Pct Recovery = 56% Analysis Date = 10/25/13 Pct Recovery = 56% Analysis Date = 10/25/13 Pct Recovery = 56% Analysis Date = 10/17/13 Pct Recovery = 56% Analysis Date = 10/17/13 Pct Recovery = 56% Analysis Date = 10/09/13 Pct Recovery = 55% Analysis Date = 10/09/13 Pct Recovery = 55% Analysis Date = 10/01/13 Pct Recovery = 55% Analysis Date = 10/01/13 Pct Recovery = 55% Analysis Date = 09/23/13 Pct Recovery = 55% Analysis Date = 09/23/13 Pct Recovery = 55% Analysis Date = 09/14/13 Pct Recovery = 55% Analysis Date = 09/14/13 Pct Recovery = 55% Analysis Date = 09/06/13 Pct Recovery = 55% Analysis Date = 09/06/13 Pct Recovery = 55% Analysis Date = 08/29/13 Pct Recovery = 55% Analysis Date = 08/29/13 Pct Recovery = 55% Analysis Date = 08/21/13 Pct Recovery = 55% Analysis Date = 08/21/13 Pct Recovery = 55% Analysis Date = 08/13/13 Pct Recovery = 55% Analysis Date = 08/13/13 Pct Recovery = 55% Analysis Date = 08/05/13 Pct Recovery = 56% Analysis Date = 08/05/13 Pct Recovery = 56% Analysis Date = 07/28/13 Pct Recovery = 56% Analysis Date = 07/28/13 Pct Recovery = 56% Analysis Date = 07/20/13 Pct Recovery = 57% Analysis Date = 07/20/13 Pct Recovery = 57% Analysis Date = 07/12/13 Pct Recovery = 57% Analysis Date = 07/12/13 Pct Recovery = 57% Analysis Date = 07/04/13 Pct Recovery = 58% Analysis Date = 07/04/13 Pct Recovery = 58% Analysis Date = 06/26/13 Pct Recovery = 58% Analysis Date = 06/26/13 Pct Recovery = 58% Analysis Date = 06/18/13 Pct Recovery = 59% Analysis Date = 06/18/13 Pct Recovery = 59% Analysis Date = 06/10/13 Pct Recovery = 59% Analysis Date = 06/10/13 Pct Recovery = 59% Analysis Date = 06/02/13 Pct Recovery = 60% Analysis Date = 06/02/13 Pct Recovery = 60% Analysis Date = 05/24/13 Pct Recovery = 60% Analysis Date = 05/24/13 Pct Recovery = 60% Analysis Date = 05/16/13 Pct Recovery = 61% Analysis Date = 05/16/13 Pct Recovery = 61% Analysis Date = 05/08/13 Pct Recovery = 61% Analysis Date = 05/08/13 Pct Recovery = 61% Analysis Date = 04/30/13 Pct Recovery = 62% Analysis Date = 04/30/13 Pct Recovery = 62% Analysis Date = 04/22/13 Pct Recovery = 62% Analysis Date = 04/22/13 Pct Recovery = 62% Analysis Date = 04/14/13 Pct Recovery = 63% Analysis Date = 04/14/13 Pct Recovery = 63% Analysis Date = 04/06/13 Pct Recovery = 64% Analysis Date = 04/06/13 Pct Recovery = 64% Analysis Date = 03/29/13 Pct Recovery = 65% Analysis Date = 03/29/13 Pct Recovery = 65% Analysis Date = 03/21/13 Pct Recovery = 66% Analysis Date = 03/21/13 Pct Recovery = 66% Analysis Date = 03/13/13 Pct Recovery = 67% Analysis Date = 03/13/13 Pct Recovery = 67% Analysis Date = 03/05/13 Pct Recovery = 68% Analysis Date = 03/05/13 Pct Recovery = 68% Analysis Date = 02/25/13 Pct Recovery = 68% Analysis Date = 02/25/13 Pct Recovery = 68% Analysis Date = 02/17/13 Pct Recovery = 69% Analysis Date = 02/17/13 Pct Recovery = 69% Analysis Date = 02/09/13 Pct Recovery = 70% Analysis Date = 02/09/13 Pct Recovery = 70% Analysis Date = 02/01/13 Pct Recovery = 71% Analysis Date = 02/01/13 Pct Recovery = 71% Analysis Date = 01/23/13 Pct Recovery = 72% Analysis Date = 01/23/13 Pct Recovery = 72% Analysis Date = 01/15/13 Pct Recovery = 73% Analysis Date = 01/15/13 Pct Recovery = 73% Analysis Date = 01/07/13 Pct Recovery = 74% Analysis Date = 01/07/13 Pct Recovery = 74% Analysis Date = 12/30/12 Pct Recovery = 75% Analysis Date = 12/30/12 Pct Recovery = 75% Analysis Date = 12/22/12 Pct Recovery = 76% Analysis Date = 12/22/12 Pct Recovery = 76% Analysis Date = 12/14/12 Pct Recovery = 77% Analysis Date = 12/14/12 Pct Recovery = 77% Analysis Date = 12/06/12 Pct Recovery = 77% Analysis Date = 12/06/12 Pct Recovery = 77% Analysis Date = 11/28/12 Pct Recovery = 78% Analysis Date = 11/28/12 Pct Recovery = 78% Analysis Date = 11/20/12 Pct Recovery = 78% Analysis Date = 11/20/12 Pct Recovery = 78% Analysis Date = 11/12/12 Pct Recovery = 79% Analysis Date = 11/12/12 Pct Recovery = 79% Analysis Date = 11/04/12 Pct Recovery = 80% Analysis Date = 11/04/12 Pct Recovery = 80% Analysis Date = 10/27/12 Pct Recovery = 80% Analysis Date = 10/27/12 Pct Recovery = 80% Analysis Date = 10/19/12 Pct Recovery = 81% Analysis Date = 10/19/12 Pct Recovery = 81% Analysis Date = 10/11/12 Pct Recovery = 81% Analysis Date = 10/11/12 Pct Recovery = 81% Analysis Date = 10/02/12 Pct Recovery = 82% Analysis Date = 10/02/12 Pct Recovery = 82% Analysis Date = 09/24/12 Pct Recovery = 83% Analysis Date = 09/24/12 Pct Recovery = 83% Analysis Date = 09/16/12 Pct Recovery = 83% Analysis Date = 09/16/12 Pct Recovery = 83% Analysis Date = 09/08/12 Pct Recovery = 84% Analysis Date = 09/08/12 Pct Recovery = 84% Analysis Date = 08/31/12 Pct Recovery = 84% Analysis Date = 08/31/12 Pct Recovery = 84% Analysis Date = 08/23/12 Pct Recovery = 84% Analysis Date = 08/23/12 Pct Recovery = 84% Analysis Date = 08/15/12 Pct Recovery = 84% Analysis Date = 08/15/12 Pct Recovery = 84% Analysis Date = 08/07/12 Pct Recovery = 84% Analysis Date = 08/07/12 Pct Recovery = 84% Analysis Date = 07/30/12 Pct Recovery = 84% Analysis Date = 07/30/12 Pct Recovery = 84% Analysis Date = 07/22/12 Pct Recovery = 84% Analysis Date = 07/22/12 Pct Recovery = 84% Analysis Date = 07/14/12 Pct Recovery = 84% Analysis Date = 07/14/12 Pct Recovery = 84% Analysis Date = 07/06/12 Pct Recovery = 84% Analysis Date = 07/06/12 Pct Recovery = 84% Analysis Date = 06/28/12 Pct Recovery = 84% Analysis Date = 06/28/12 Pct Recovery = 84% Analysis Date = 06/20/12 Pct Recovery = 84% Analysis Date = 06/20/12 Pct Recovery = 84% Analysis Date = 06/11/12 Pct Recovery = 84% Analysis Date = 06/11/12 Pct Recovery = 84% Analysis Date = 06/03/12 Pct Recovery = 84% Analysis Date = 06/03/12 Pct Recovery = 84% Analysis Date = 05/26/12 Pct Recovery = 84% Analysis Date = 05/26/12 Pct Recovery = 84% Analysis Date = 05/18/12 Pct Recovery = 84% Analysis Date = 05/18/12 Pct Recovery = 84% Analysis Date = 05/10/12 Pct Recovery = 84% Analysis Date = 05/10/12 Pct Recovery = 84% Analysis Date = 05/02/12 Pct Recovery = 84% Analysis Date = 05/02/12 Pct Recovery = 84% Analysis Date = 04/24/12 Pct Recovery = 83% Analysis Date = 04/24/12 Pct Recovery = 83% Analysis Date = 04/16/12 Pct Recovery = 83% Analysis Date = 04/16/12 Pct Recovery = 83% Analysis Date = 04/08/12 Pct Recovery = 83% Analysis Date = 04/08/12 Pct Recovery = 83% Analysis Date = 03/31/12 Pct Recovery = 83% Analysis Date = 03/31/12 Pct Recovery = 83% Analysis Date = 03/23/12 Pct Recovery = 83% Analysis Date = 03/23/12 Pct Recovery = 83% Analysis Date = 03/15/12 Pct Recovery = 83% Analysis Date = 03/15/12 Pct Recovery = 83% Analysis Date = 03/07/12 Pct Recovery = 83% Analysis Date = 03/07/12 Pct Recovery = 83% Analysis Date = 02/28/12 Pct Recovery = 83% Analysis Date = 02/28/12 Pct Recovery = 83% Analysis Date = 02/20/12 Pct Recovery = 83% Analysis Date = 02/20/12 Pct Recovery = 83% Analysis Date = 02/11/12 Pct Recovery = 83% Analysis Date = 02/11/12 Pct Recovery = 83% Analysis Date = 02/03/12 Pct Recovery = 83% Analysis Date = 02/03/12 Pct Recovery = 83% Analysis Date = 01/26/12 Pct Recovery = 83% Analysis Date = 01/26/12 Pct Recovery = 83% Analysis Date = 01/18/12 Pct Recovery = 83% Analysis Date = 01/18/12 Pct Recovery = 83% Analysis Date = 01/10/12 Pct Recovery = 83% Analysis Date = 01/10/12 Pct Recovery = 83% Analysis Date = 01/02/12 Pct Recovery = 83% Analysis Date = 01/02/12 Pct Recovery = 83% Analysis Date = 12/25/11 Pct Recovery = 83% Analysis Date = 12/25/11 Pct Recovery = 83% Analysis Date = 12/17/11 Pct Recovery = 83% Analysis Date = 12/17/11 Pct Recovery = 83% Analysis Date = 12/09/11 Pct Recovery = 82% Analysis Date = 12/09/11 Pct Recovery = 82% Analysis Date = 12/01/11 Pct Recovery = 82% Analysis Date = 12/01/11 Pct Recovery = 82% Analysis Date = 11/23/11 Pct Recovery = 82% Analysis Date = 11/23/11 Pct Recovery = 82% Analysis Date = 11/15/11 Pct Recovery = 82% Analysis Date = 11/15/11 Pct Recovery = 82% Analysis Date = 11/07/11 Pct Recovery = 82% Analysis Date = 11/07/11 Pct Recovery = 82% Analysis Date = 10/30/11 Pct Recovery = 82% Analysis Date = 10/30/11 Pct Recovery = 82% Analysis Date = 10/21/11 Pct Recovery = 82% Analysis Date = 10/21/11 Pct Recovery = 82% Analysis Date = 10/13/11 Pct Recovery = 82% Analysis Date = 10/13/11 Pct Recovery = 82% Analysis Date = 10/05/11 Pct Recovery = 82% Analysis Date = 10/05/11 Pct Recovery = 82% Analysis Date = 09/27/11 Pct Recovery = 82% Analysis Date = 09/27/11 Pct Recovery = 82% Analysis Date = 09/19/11 Pct Recovery = 82% Analysis Date = 09/19/11 Pct Recovery = 82% Analysis Date = 09/11/11 Pct Recovery = 82% Analysis Date = 09/11/11 Pct Recovery = 82% Analysis Date = 09/03/11 Pct Recovery = 81% Analysis Date = 09/03/11 Pct Recovery = 81% Analysis Date = 08/26/11 Pct Recovery = 81% Analysis Date = 08/26/11 Pct Recovery = 81% Analysis Date = 08/18/11 Pct Recovery = 81% Analysis Date = 08/18/11 Pct Recovery = 81% Analysis Date = 08/10/11 Pct Recovery = 81% Analysis Date = 08/10/11 Pct Recovery = 81% Analysis Date = 08/02/11 Pct Recovery = 81% Analysis Date = 08/02/11 Pct Recovery = 81% Analysis Date = 07/25/11 Pct Recovery = 81% Analysis Date = 07/25/11 Pct Recovery = 81% Analysis Date = 07/17/11 Pct Recovery = 81% Analysis Date = 07/17/11 Pct Recovery = 81% Analysis Date = 07/09/11 Pct Recovery = 80% Analysis Date = 07/09/11 Pct Recovery = 80% Analysis Date = 06/30/11 Pct Recovery = 80% Analysis Date = 06/30/11 Pct Recovery = 80% Analysis Date = 06/22/11 Pct Recovery = 80% Analysis Date = 06/22/11 Pct Recovery = 80% Analysis Date = 06/14/11 Pct Recovery = 80% Analysis Date = 06/14/11 Pct Recovery = 80% Analysis Date = 06/06/11 Pct Recovery = 80% Analysis Date = 06/06/11 Pct Recovery = 80% Analysis Date = 05/29/11 Pct Recovery = 80% Analysis Date = 05/29/11 Pct Recovery = 80% Analysis Date = 05/21/11 Pct Recovery = 79% Analysis Date = 05/21/11 Pct Recovery = 79% Analysis Date = 05/13/11 Pct Recovery = 79% Analysis Date = 05/13/11 Pct Recovery = 79% Analysis Date = 05/05/11 Pct Recovery = 79% Analysis Date = 05/05/11 Pct Recovery = 79% Analysis Date = 04/27/11 Pct Recovery = 79% Analysis Date = 04/27/11 Pct Recovery = 79% Analysis Date = 04/19/11 Pct Recovery = 79% Analysis Date = 04/19/11 Pct Recovery = 79% Analysis Date = 04/11/11 Pct Recovery = 78% Analysis Date = 04/11/11 Pct Recovery = 78% Analysis Date = 04/03/11 Pct Recovery = 78% Analysis Date = 04/03/11 Pct Recovery = 78% Analysis Date = 03/26/11 Pct Recovery = 78% Analysis Date = 03/26/11 Pct Recovery = 78% Analysis Date = 03/18/11 Pct Recovery = 78% Analysis Date = 03/18/11 Pct Recovery = 78% Analysis Date = 03/10/11 Pct Recovery = 78% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
4-ANDROSTENE-3,17-DIONE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 35 69% 19% 70% 19%
Total 35 69% 19% 70% 19%

Sample Statistics
4-ANDROSTENE-3,17-DIONE

Characteristic N % % Basis
Plotted 35 80% Spiked
Estimated Values 0 0% Spiked
Deleted Values 2 2% Spiked + Not Spiked
Spiked, Censored 3 7% Spiked
Spiked 46 .  
False Negatives 6 14% 6 out of 44
Not Spiked 85 .  
False Positives 1 1% 1 out of 85

BQS OBSP Determination:
BISPHENOL A
METHOD: 4434 , TESTIDCODE: 67305GM005
Open Data Set

Analysis Date = 05/09/11 SpikeMix = Abs 081810: 100 µl Pct Recovery = 73% Analysis Date = 02/01/12 SpikeMix = Spex Organics T1100629008: 100 µl Pct Recovery = 84% Analysis Date = 09/29/11 SpikeMix = Spex Organics T1100629008: 100 µl Pct Recovery = 93% Analysis Date = 03/31/11 SpikeMix = Spex Organics T1100629008: 100 µl Pct Recovery = 73% Analysis Date = 07/02/12 SpikeMix = Abs 081810: 100 µl Pct Recovery = 87% Analysis Date = 04/17/12 SpikeMix = Abs 081810: 100 µl Pct Recovery = 103% Analysis Date = 10/03/11 SpikeMix = Abs 081810: 100 µl Pct Recovery = 80% Analysis Date = 03/14/14 SpikeMix = Supelco LB99393: 50 µl & Abs 050813: 50 µl Pct Recovery = 101% Analysis Date = 02/25/14 SpikeMix = ERA 0415-13-01.1A: 50 µl & Abs 050813: 50 µl Pct Recovery = 81% Analysis Date = 03/14/14 SpikeMix = ERA 0415-13-01.2A: 50 µl & Spex Organics T1130423008: 50 µl Pct Recovery = 63% Analysis Date = 03/05/14 SpikeMix = Spex Organics T1130423008: 50 µl & Abs 071513: 50 µl Pct Recovery = 66% Analysis Date = 08/09/13 SpikeMix = ERA 0415-13-01.2A: 50 µl & Spex Organics T1130423008: 50 µl Pct Recovery = 152% Analysis Date = 05/26/11 SpikeMix = Spex Organics T1100629008: 25 µl Pct Recovery = 67% Analysis Date = 08/16/12 SpikeMix = Spex Organics T1100629008: 25 µl Pct Recovery = 69% Analysis Date = 11/28/11 SpikeMix = Spex Organics T1100629008: 25 µl Pct Recovery = 79% Analysis Date = 10/13/11 SpikeMix = Spex Organics T1100629008: 25 µl Pct Recovery = 62% Analysis Date = 03/27/12 SpikeMix = Abs 081810: 25 µl Pct Recovery = 91% Analysis Date = 01/27/12 SpikeMix = Abs 081810: 25 µl Pct Recovery = 65% Analysis Date = 10/12/11 SpikeMix = Abs 081810: 25 µl Pct Recovery = 74% Analysis Date = 03/10/11 SpikeMix = Spex Organics T1100629008: 25 µl Pct Recovery = 59% Analysis Date = 07/11/11 SpikeMix = Spex Organics T1100629008: 25 µl Pct Recovery = 44% Analysis Date = 06/13/11 SpikeMix = Abs 081810: 25 µl Pct Recovery = 47% Analysis Date = 03/30/11 SpikeMix = Abs 081810: 25 µl Pct Recovery = 73% Analysis Date = 12/03/12 SpikeMix = ERA 0511-12-02: 50 µl & Abs 051512: 50 µl Pct Recovery = 53% Analysis Date = 08/31/16 SpikeMix = Spex Organics TS160420010: 50 µl & ChemService 5016200: 50 µl Pct Recovery = 78% Analysis Date = 12/15/16 SpikeMix = Abs 061416H: 50 µl & ChemService 5016100: 50 µl Pct Recovery = 74% Analysis Date = 04/13/15 SpikeMix = Abs 042114: 60 µl & Spex Organics E1140505004: 60 µl Pct Recovery = 94% Analysis Date = 02/12/15 SpikeMix = Supelco LC06946: 60 µl & Abs 042114: 60 µl Pct Recovery = 96% Analysis Date = 08/26/14 SpikeMix = Abs 031014: 60 µl & Abs 042114: 60 µl Pct Recovery = 59% Analysis Date = 08/22/14 SpikeMix = ERA 0227-14-07.2: 60 µl & Abs 042114: 60 µl Pct Recovery = 57% Analysis Date = 04/01/15 SpikeMix = ERA 0227-14-07.2: 60 µl & ChemService 2561700: 60 µl Pct Recovery = 60% Analysis Date = 01/21/15 SpikeMix = ChemService 2561700: 60 µl & Spex Organics E1140505004: 60 µl Pct Recovery = 94% Analysis Date = 09/23/14 SpikeMix = Supelco LC06946: 60 µl & ChemService 2561700: 60 µl Pct Recovery = 90% Analysis Date = 05/06/14 SpikeMix = Abs 031014: 60 µl & ChemService 2561700: 60 µl Pct Recovery = 57% Analysis Date = 01/05/16 SpikeMix = Supelco LC13547: 60 µl & ChemService 4073900: 60 µl Pct Recovery = 93% Analysis Date = 01/08/16 SpikeMix = Spex Organics EN150501025: 60 µl & ERA 0601-15-04: 60 µl Pct Recovery = 43% Analysis Date = 07/21/15 SpikeMix = Supelco LC13547: 50 µl & Spex Organics EN150501025: 50 µl Pct Recovery = 104% Analysis Date = 01/13/17 SpikeMix = Abs 052616: 30 µl & ChemService 5016200: 30 µl Pct Recovery = 66% Analysis Date = 09/21/16 SpikeMix = ChemService 5016200: 30 µl & ChemService 5016100: 30 µl Pct Recovery = 96% Analysis Date = 09/16/16 SpikeMix = Spex Organics EN160621015: 30 µl & ChemService 5016200: 30 µl Pct Recovery = 73% Analysis Date = 09/09/16 SpikeMix = ChemService 5016200: 30 µl & Supelco LC20140V: 30 µl Pct Recovery = 71% Analysis Date = 07/12/16 SpikeMix = Spex Organics EN150501025: 50 µl & ERA 0601-15-04: 50 µl Pct Recovery = 55% Analysis Date = 06/24/16 SpikeMix = ERA 0601-15-04: 50 µl & ChemService 4073900: 50 µl Pct Recovery = 135% Analysis Date = 03/07/16 SpikeMix = Abs 041515: 50 µl & ERA 0601-15-04: 50 µl Pct Recovery = 40% Analysis Date = 12/10/15 SpikeMix = Abs 041515: 50 µl & ERA 0601-15-04: 50 µl Pct Recovery = 112% Analysis Date = 09/14/15 SpikeMix = ERA 0601-15-04: 50 µl & ChemService 4073900: 50 µl Pct Recovery = 80% Analysis Date = 08/10/15 SpikeMix = ERA 0601-15-04: 50 µl & Crescent 04EE007: 50 µl Pct Recovery = 60% Analysis Date = 12/05/16 SpikeMix = Abs 052616: 30 µl & Abs 061416H: 30 µl Pct Recovery = 70% Analysis Date = 04/03/13 SpikeMix = Spex Organics T1120525010: 25 µl & Abs 051512: 25 µl Pct Recovery = 63% Analysis Date = 11/01/12 SpikeMix = ERA 0507-12-04.1: 25 µl & Abs 051512: 25 µl Pct Recovery = 59% Analysis Date = 08/31/12 SpikeMix = ERA 0511-12-02: 25 µl & Abs 051512: 25 µl Pct Recovery = 67% Analysis Date = 08/24/12 SpikeMix = Abs 051512: 25 µl Pct Recovery = 89% Analysis Date = 12/22/14 SpikeMix = Abs 042114: 30 µl & Abs 031014: 30 µl Pct Recovery = 120% Analysis Date = 12/16/14 SpikeMix = Supelco LC06946: 30 µl & Abs 042114: 30 µl Pct Recovery = 67% Analysis Date = 11/05/14 SpikeMix = ERA 0227-14-07.2: 30 µl & Abs 042114: 30 µl Pct Recovery = 76% Analysis Date = 03/03/14 SpikeMix = Abs 050813: 20 µl & Abs 071513: 20 µl Pct Recovery = 88% Analysis Date = 02/19/14 SpikeMix = Abs 050813: 20 µl & Abs 071513: 20 µl Pct Recovery = 73% Analysis Date = 11/18/13 SpikeMix = ERA 0415-13-01.2A: 20 µl & Abs 050813: 20 µl Pct Recovery = 84% Analysis Date = 04/01/15 SpikeMix = ChemService 2561700: 30 µl & Spex Organics E1140505004: 30 µl Pct Recovery = 50% Analysis Date = 01/21/15 SpikeMix = Supelco LC06946: 30 µl & ChemService 2561700: 30 µl Pct Recovery = 50% Analysis Date = 07/28/14 SpikeMix = ERA 0227-14-07.2: 30 µl & ChemService 2561700: 30 µl Pct Recovery = 59% Analysis Date = 12/09/13 SpikeMix = Supelco LB99393: 20 µl & Spex Organics T1130423008: 20 µl Pct Recovery = 53% Analysis Date = 06/27/13 SpikeMix = ERA 0415-13-01.1A: 20 µl & Spex Organics T1130423008: 20 µl Pct Recovery = 59% Analysis Date = 06/04/13 SpikeMix = Supelco LB99393: 20 µl & Spex Organics T1130423008: 20 µl Pct Recovery = 110% Analysis Date = 03/18/16 SpikeMix = Supelco LC13547: 30 µl & ChemService 4073900: 30 µl Pct Recovery = 80% Analysis Date = 03/18/16 SpikeMix = Spex Organics EN150501025: 30 µl & Supelco LC13547: 30 µl Pct Recovery = 80% Analysis Date = 11/02/15 SpikeMix = Supelco LC13547: 30 µl & Crescent 04EE007: 30 µl Pct Recovery = 87% Analysis Date = 09/17/15 SpikeMix = Supelco LC13547: 30 µl & Spex Organics EN150501025: 30 µl Pct Recovery = 100% Analysis Date = 09/17/15 SpikeMix = Supelco LC13547: 30 µl & Abs 041515: 30 µl Pct Recovery = 107% Analysis Date = 06/29/15 SpikeMix = Supelco LC13547: 30 µl & Abs 041515: 30 µl Pct Recovery = 73% Analysis Date = 01/08/16 SpikeMix = ERA 0601-15-04: 30 µl & ChemService 4073900: 30 µl Pct Recovery = 87% Analysis Date = 01/13/17 Pct Recovery = 77% Analysis Date = 01/02/17 Pct Recovery = 77% Analysis Date = 01/02/17 Pct Recovery = 77% Analysis Date = 12/22/16 Pct Recovery = 77% Analysis Date = 12/22/16 Pct Recovery = 77% Analysis Date = 12/11/16 Pct Recovery = 77% Analysis Date = 12/11/16 Pct Recovery = 77% Analysis Date = 12/01/16 Pct Recovery = 77% Analysis Date = 12/01/16 Pct Recovery = 77% Analysis Date = 11/20/16 Pct Recovery = 78% Analysis Date = 11/20/16 Pct Recovery = 78% Analysis Date = 11/09/16 Pct Recovery = 78% Analysis Date = 11/09/16 Pct Recovery = 78% Analysis Date = 10/30/16 Pct Recovery = 78% Analysis Date = 10/30/16 Pct Recovery = 78% Analysis Date = 10/19/16 Pct Recovery = 78% Analysis Date = 10/19/16 Pct Recovery = 78% Analysis Date = 10/08/16 Pct Recovery = 78% Analysis Date = 10/08/16 Pct Recovery = 78% Analysis Date = 09/28/16 Pct Recovery = 78% Analysis Date = 09/28/16 Pct Recovery = 78% Analysis Date = 09/17/16 Pct Recovery = 78% Analysis Date = 09/17/16 Pct Recovery = 78% Analysis Date = 09/06/16 Pct Recovery = 78% Analysis Date = 09/06/16 Pct Recovery = 78% Analysis Date = 08/27/16 Pct Recovery = 78% Analysis Date = 08/27/16 Pct Recovery = 78% Analysis Date = 08/16/16 Pct Recovery = 79% Analysis Date = 08/16/16 Pct Recovery = 79% Analysis Date = 08/05/16 Pct Recovery = 79% Analysis Date = 08/05/16 Pct Recovery = 79% Analysis Date = 07/26/16 Pct Recovery = 79% Analysis Date = 07/26/16 Pct Recovery = 79% Analysis Date = 07/15/16 Pct Recovery = 79% Analysis Date = 07/15/16 Pct Recovery = 79% Analysis Date = 07/04/16 Pct Recovery = 79% Analysis Date = 07/04/16 Pct Recovery = 79% Analysis Date = 06/24/16 Pct Recovery = 79% Analysis Date = 06/24/16 Pct Recovery = 79% Analysis Date = 06/13/16 Pct Recovery = 79% Analysis Date = 06/13/16 Pct Recovery = 79% Analysis Date = 06/02/16 Pct Recovery = 79% Analysis Date = 06/02/16 Pct Recovery = 79% Analysis Date = 05/23/16 Pct Recovery = 79% Analysis Date = 05/23/16 Pct Recovery = 79% Analysis Date = 05/12/16 Pct Recovery = 79% Analysis Date = 05/12/16 Pct Recovery = 79% Analysis Date = 05/01/16 Pct Recovery = 79% Analysis Date = 05/01/16 Pct Recovery = 79% Analysis Date = 04/21/16 Pct Recovery = 79% Analysis Date = 04/21/16 Pct Recovery = 79% Analysis Date = 04/10/16 Pct Recovery = 80% Analysis Date = 04/10/16 Pct Recovery = 80% Analysis Date = 03/30/16 Pct Recovery = 80% Analysis Date = 03/30/16 Pct Recovery = 80% Analysis Date = 03/19/16 Pct Recovery = 80% Analysis Date = 03/19/16 Pct Recovery = 80% Analysis Date = 03/09/16 Pct Recovery = 80% Analysis Date = 03/09/16 Pct Recovery = 80% Analysis Date = 02/27/16 Pct Recovery = 80% Analysis Date = 02/27/16 Pct Recovery = 80% Analysis Date = 02/16/16 Pct Recovery = 80% Analysis Date = 02/16/16 Pct Recovery = 80% Analysis Date = 02/06/16 Pct Recovery = 80% Analysis Date = 02/06/16 Pct Recovery = 80% Analysis Date = 01/26/16 Pct Recovery = 80% Analysis Date = 01/26/16 Pct Recovery = 80% Analysis Date = 01/15/16 Pct Recovery = 80% Analysis Date = 01/15/16 Pct Recovery = 80% Analysis Date = 01/05/16 Pct Recovery = 80% Analysis Date = 01/05/16 Pct Recovery = 80% Analysis Date = 12/25/15 Pct Recovery = 80% Analysis Date = 12/25/15 Pct Recovery = 80% Analysis Date = 12/14/15 Pct Recovery = 80% Analysis Date = 12/14/15 Pct Recovery = 80% Analysis Date = 12/04/15 Pct Recovery = 80% Analysis Date = 12/04/15 Pct Recovery = 80% Analysis Date = 11/23/15 Pct Recovery = 80% Analysis Date = 11/23/15 Pct Recovery = 80% Analysis Date = 11/12/15 Pct Recovery = 80% Analysis Date = 11/12/15 Pct Recovery = 80% Analysis Date = 11/02/15 Pct Recovery = 81% Analysis Date = 11/02/15 Pct Recovery = 81% Analysis Date = 10/22/15 Pct Recovery = 81% Analysis Date = 10/22/15 Pct Recovery = 81% Analysis Date = 10/11/15 Pct Recovery = 81% Analysis Date = 10/11/15 Pct Recovery = 81% Analysis Date = 10/01/15 Pct Recovery = 81% Analysis Date = 10/01/15 Pct Recovery = 81% Analysis Date = 09/20/15 Pct Recovery = 81% Analysis Date = 09/20/15 Pct Recovery = 81% Analysis Date = 09/09/15 Pct Recovery = 81% Analysis Date = 09/09/15 Pct Recovery = 81% Analysis Date = 08/30/15 Pct Recovery = 81% Analysis Date = 08/30/15 Pct Recovery = 81% Analysis Date = 08/19/15 Pct Recovery = 81% Analysis Date = 08/19/15 Pct Recovery = 81% Analysis Date = 08/08/15 Pct Recovery = 81% Analysis Date = 08/08/15 Pct Recovery = 81% Analysis Date = 07/29/15 Pct Recovery = 81% Analysis Date = 07/29/15 Pct Recovery = 81% Analysis Date = 07/18/15 Pct Recovery = 81% Analysis Date = 07/18/15 Pct Recovery = 81% Analysis Date = 07/07/15 Pct Recovery = 80% Analysis Date = 07/07/15 Pct Recovery = 80% Analysis Date = 06/26/15 Pct Recovery = 80% Analysis Date = 06/26/15 Pct Recovery = 80% Analysis Date = 06/16/15 Pct Recovery = 80% Analysis Date = 06/16/15 Pct Recovery = 80% Analysis Date = 06/05/15 Pct Recovery = 80% Analysis Date = 06/05/15 Pct Recovery = 80% Analysis Date = 05/25/15 Pct Recovery = 80% Analysis Date = 05/25/15 Pct Recovery = 80% Analysis Date = 05/15/15 Pct Recovery = 80% Analysis Date = 05/15/15 Pct Recovery = 80% Analysis Date = 05/04/15 Pct Recovery = 79% Analysis Date = 05/04/15 Pct Recovery = 79% Analysis Date = 04/23/15 Pct Recovery = 79% Analysis Date = 04/23/15 Pct Recovery = 79% Analysis Date = 04/13/15 Pct Recovery = 79% Analysis Date = 04/13/15 Pct Recovery = 79% Analysis Date = 04/02/15 Pct Recovery = 79% Analysis Date = 04/02/15 Pct Recovery = 79% Analysis Date = 03/22/15 Pct Recovery = 79% Analysis Date = 03/22/15 Pct Recovery = 79% Analysis Date = 03/12/15 Pct Recovery = 79% Analysis Date = 03/12/15 Pct Recovery = 79% Analysis Date = 03/01/15 Pct Recovery = 78% Analysis Date = 03/01/15 Pct Recovery = 78% Analysis Date = 02/18/15 Pct Recovery = 78% Analysis Date = 02/18/15 Pct Recovery = 78% Analysis Date = 02/08/15 Pct Recovery = 78% Analysis Date = 02/08/15 Pct Recovery = 78% Analysis Date = 01/28/15 Pct Recovery = 78% Analysis Date = 01/28/15 Pct Recovery = 78% Analysis Date = 01/17/15 Pct Recovery = 78% Analysis Date = 01/17/15 Pct Recovery = 78% Analysis Date = 01/07/15 Pct Recovery = 78% Analysis Date = 01/07/15 Pct Recovery = 78% Analysis Date = 12/27/14 Pct Recovery = 78% Analysis Date = 12/27/14 Pct Recovery = 78% Analysis Date = 12/16/14 Pct Recovery = 78% Analysis Date = 12/16/14 Pct Recovery = 78% Analysis Date = 12/06/14 Pct Recovery = 78% Analysis Date = 12/06/14 Pct Recovery = 78% Analysis Date = 11/25/14 Pct Recovery = 78% Analysis Date = 11/25/14 Pct Recovery = 78% Analysis Date = 11/14/14 Pct Recovery = 78% Analysis Date = 11/14/14 Pct Recovery = 78% Analysis Date = 11/04/14 Pct Recovery = 78% Analysis Date = 11/04/14 Pct Recovery = 78% Analysis Date = 10/24/14 Pct Recovery = 78% Analysis Date = 10/24/14 Pct Recovery = 78% Analysis Date = 10/13/14 Pct Recovery = 78% Analysis Date = 10/13/14 Pct Recovery = 78% Analysis Date = 10/02/14 Pct Recovery = 78% Analysis Date = 10/02/14 Pct Recovery = 78% Analysis Date = 09/22/14 Pct Recovery = 78% Analysis Date = 09/22/14 Pct Recovery = 78% Analysis Date = 09/11/14 Pct Recovery = 78% Analysis Date = 09/11/14 Pct Recovery = 78% Analysis Date = 08/31/14 Pct Recovery = 78% Analysis Date = 08/31/14 Pct Recovery = 78% Analysis Date = 08/21/14 Pct Recovery = 78% Analysis Date = 08/21/14 Pct Recovery = 78% Analysis Date = 08/10/14 Pct Recovery = 78% Analysis Date = 08/10/14 Pct Recovery = 78% Analysis Date = 07/30/14 Pct Recovery = 78% Analysis Date = 07/30/14 Pct Recovery = 78% Analysis Date = 07/20/14 Pct Recovery = 78% Analysis Date = 07/20/14 Pct Recovery = 78% Analysis Date = 07/09/14 Pct Recovery = 78% Analysis Date = 07/09/14 Pct Recovery = 78% Analysis Date = 06/28/14 Pct Recovery = 78% Analysis Date = 06/28/14 Pct Recovery = 78% Analysis Date = 06/18/14 Pct Recovery = 78% Analysis Date = 06/18/14 Pct Recovery = 78% Analysis Date = 06/07/14 Pct Recovery = 78% Analysis Date = 06/07/14 Pct Recovery = 78% Analysis Date = 05/27/14 Pct Recovery = 78% Analysis Date = 05/27/14 Pct Recovery = 78% Analysis Date = 05/17/14 Pct Recovery = 78% Analysis Date = 05/17/14 Pct Recovery = 78% Analysis Date = 05/06/14 Pct Recovery = 78% Analysis Date = 05/06/14 Pct Recovery = 78% Analysis Date = 04/25/14 Pct Recovery = 78% Analysis Date = 04/25/14 Pct Recovery = 78% Analysis Date = 04/15/14 Pct Recovery = 78% Analysis Date = 04/15/14 Pct Recovery = 78% Analysis Date = 04/04/14 Pct Recovery = 78% Analysis Date = 04/04/14 Pct Recovery = 78% Analysis Date = 03/24/14 Pct Recovery = 78% Analysis Date = 03/24/14 Pct Recovery = 78% Analysis Date = 03/14/14 Pct Recovery = 78% Analysis Date = 03/14/14 Pct Recovery = 78% Analysis Date = 03/03/14 Pct Recovery = 78% Analysis Date = 03/03/14 Pct Recovery = 78% Analysis Date = 02/20/14 Pct Recovery = 78% Analysis Date = 02/20/14 Pct Recovery = 78% Analysis Date = 02/10/14 Pct Recovery = 78% Analysis Date = 02/10/14 Pct Recovery = 78% Analysis Date = 01/30/14 Pct Recovery = 78% Analysis Date = 01/30/14 Pct Recovery = 78% Analysis Date = 01/19/14 Pct Recovery = 78% Analysis Date = 01/19/14 Pct Recovery = 78% Analysis Date = 01/08/14 Pct Recovery = 78% Analysis Date = 01/08/14 Pct Recovery = 78% Analysis Date = 12/29/13 Pct Recovery = 78% Analysis Date = 12/29/13 Pct Recovery = 78% Analysis Date = 12/18/13 Pct Recovery = 78% Analysis Date = 12/18/13 Pct Recovery = 78% Analysis Date = 12/07/13 Pct Recovery = 77% Analysis Date = 12/07/13 Pct Recovery = 77% Analysis Date = 11/27/13 Pct Recovery = 77% Analysis Date = 11/27/13 Pct Recovery = 77% Analysis Date = 11/16/13 Pct Recovery = 77% Analysis Date = 11/16/13 Pct Recovery = 77% Analysis Date = 11/05/13 Pct Recovery = 77% Analysis Date = 11/05/13 Pct Recovery = 77% Analysis Date = 10/26/13 Pct Recovery = 78% Analysis Date = 10/26/13 Pct Recovery = 78% Analysis Date = 10/15/13 Pct Recovery = 78% Analysis Date = 10/15/13 Pct Recovery = 78% Analysis Date = 10/04/13 Pct Recovery = 78% Analysis Date = 10/04/13 Pct Recovery = 78% Analysis Date = 09/24/13 Pct Recovery = 78% Analysis Date = 09/24/13 Pct Recovery = 78% Analysis Date = 09/13/13 Pct Recovery = 78% Analysis Date = 09/13/13 Pct Recovery = 78% Analysis Date = 09/02/13 Pct Recovery = 78% Analysis Date = 09/02/13 Pct Recovery = 78% Analysis Date = 08/23/13 Pct Recovery = 78% Analysis Date = 08/23/13 Pct Recovery = 78% Analysis Date = 08/12/13 Pct Recovery = 78% Analysis Date = 08/12/13 Pct Recovery = 78% Analysis Date = 08/01/13 Pct Recovery = 78% Analysis Date = 08/01/13 Pct Recovery = 78% Analysis Date = 07/22/13 Pct Recovery = 78% Analysis Date = 07/22/13 Pct Recovery = 78% Analysis Date = 07/11/13 Pct Recovery = 78% Analysis Date = 07/11/13 Pct Recovery = 78% Analysis Date = 06/30/13 Pct Recovery = 78% Analysis Date = 06/30/13 Pct Recovery = 78% Analysis Date = 06/20/13 Pct Recovery = 78% Analysis Date = 06/20/13 Pct Recovery = 78% Analysis Date = 06/09/13 Pct Recovery = 78% Analysis Date = 06/09/13 Pct Recovery = 78% Analysis Date = 05/29/13 Pct Recovery = 78% Analysis Date = 05/29/13 Pct Recovery = 78% Analysis Date = 05/19/13 Pct Recovery = 78% Analysis Date = 05/19/13 Pct Recovery = 78% Analysis Date = 05/08/13 Pct Recovery = 78% Analysis Date = 05/08/13 Pct Recovery = 78% Analysis Date = 04/27/13 Pct Recovery = 78% Analysis Date = 04/27/13 Pct Recovery = 78% Analysis Date = 04/16/13 Pct Recovery = 78% Analysis Date = 04/16/13 Pct Recovery = 78% Analysis Date = 04/06/13 Pct Recovery = 78% Analysis Date = 04/06/13 Pct Recovery = 78% Analysis Date = 03/26/13 Pct Recovery = 78% Analysis Date = 03/26/13 Pct Recovery = 78% Analysis Date = 03/15/13 Pct Recovery = 78% Analysis Date = 03/15/13 Pct Recovery = 78% Analysis Date = 03/05/13 Pct Recovery = 78% Analysis Date = 03/05/13 Pct Recovery = 78% Analysis Date = 02/22/13 Pct Recovery = 78% Analysis Date = 02/22/13 Pct Recovery = 78% Analysis Date = 02/11/13 Pct Recovery = 78% Analysis Date = 02/11/13 Pct Recovery = 78% Analysis Date = 02/01/13 Pct Recovery = 78% Analysis Date = 02/01/13 Pct Recovery = 78% Analysis Date = 01/21/13 Pct Recovery = 78% Analysis Date = 01/21/13 Pct Recovery = 78% Analysis Date = 01/10/13 Pct Recovery = 78% Analysis Date = 01/10/13 Pct Recovery = 78% Analysis Date = 12/31/12 Pct Recovery = 78% Analysis Date = 12/31/12 Pct Recovery = 78% Analysis Date = 12/20/12 Pct Recovery = 78% Analysis Date = 12/20/12 Pct Recovery = 78% Analysis Date = 12/09/12 Pct Recovery = 78% Analysis Date = 12/09/12 Pct Recovery = 78% Analysis Date = 11/29/12 Pct Recovery = 77% Analysis Date = 11/29/12 Pct Recovery = 77% Analysis Date = 11/18/12 Pct Recovery = 77% Analysis Date = 11/18/12 Pct Recovery = 77% Analysis Date = 11/07/12 Pct Recovery = 77% Analysis Date = 11/07/12 Pct Recovery = 77% Analysis Date = 10/28/12 Pct Recovery = 77% Analysis Date = 10/28/12 Pct Recovery = 77% Analysis Date = 10/17/12 Pct Recovery = 77% Analysis Date = 10/17/12 Pct Recovery = 77% Analysis Date = 10/06/12 Pct Recovery = 77% Analysis Date = 10/06/12 Pct Recovery = 77% Analysis Date = 09/26/12 Pct Recovery = 77% Analysis Date = 09/26/12 Pct Recovery = 77% Analysis Date = 09/15/12 Pct Recovery = 77% Analysis Date = 09/15/12 Pct Recovery = 77% Analysis Date = 09/04/12 Pct Recovery = 77% Analysis Date = 09/04/12 Pct Recovery = 77% Analysis Date = 08/25/12 Pct Recovery = 77% Analysis Date = 08/25/12 Pct Recovery = 77% Analysis Date = 08/14/12 Pct Recovery = 76% Analysis Date = 08/14/12 Pct Recovery = 76% Analysis Date = 08/03/12 Pct Recovery = 76% Analysis Date = 08/03/12 Pct Recovery = 76% Analysis Date = 07/23/12 Pct Recovery = 76% Analysis Date = 07/23/12 Pct Recovery = 76% Analysis Date = 07/13/12 Pct Recovery = 76% Analysis Date = 07/13/12 Pct Recovery = 76% Analysis Date = 07/02/12 Pct Recovery = 76% Analysis Date = 07/02/12 Pct Recovery = 76% Analysis Date = 06/21/12 Pct Recovery = 76% Analysis Date = 06/21/12 Pct Recovery = 76% Analysis Date = 06/11/12 Pct Recovery = 75% Analysis Date = 06/11/12 Pct Recovery = 75% Analysis Date = 05/31/12 Pct Recovery = 75% Analysis Date = 05/31/12 Pct Recovery = 75% Analysis Date = 05/20/12 Pct Recovery = 75% Analysis Date = 05/20/12 Pct Recovery = 75% Analysis Date = 05/10/12 Pct Recovery = 75% Analysis Date = 05/10/12 Pct Recovery = 75% Analysis Date = 04/29/12 Pct Recovery = 75% Analysis Date = 04/29/12 Pct Recovery = 75% Analysis Date = 04/18/12 Pct Recovery = 75% Analysis Date = 04/18/12 Pct Recovery = 75% Analysis Date = 04/08/12 Pct Recovery = 75% Analysis Date = 04/08/12 Pct Recovery = 75% Analysis Date = 03/28/12 Pct Recovery = 74% Analysis Date = 03/28/12 Pct Recovery = 74% Analysis Date = 03/17/12 Pct Recovery = 74% Analysis Date = 03/17/12 Pct Recovery = 74% Analysis Date = 03/07/12 Pct Recovery = 74% Analysis Date = 03/07/12 Pct Recovery = 74% Analysis Date = 02/25/12 Pct Recovery = 74% Analysis Date = 02/25/12 Pct Recovery = 74% Analysis Date = 02/14/12 Pct Recovery = 74% Analysis Date = 02/14/12 Pct Recovery = 74% Analysis Date = 02/04/12 Pct Recovery = 74% Analysis Date = 02/04/12 Pct Recovery = 74% Analysis Date = 01/24/12 Pct Recovery = 73% Analysis Date = 01/24/12 Pct Recovery = 73% Analysis Date = 01/13/12 Pct Recovery = 73% Analysis Date = 01/13/12 Pct Recovery = 73% Analysis Date = 01/03/12 Pct Recovery = 73% Analysis Date = 01/03/12 Pct Recovery = 73% Analysis Date = 12/23/11 Pct Recovery = 73% Analysis Date = 12/23/11 Pct Recovery = 73% Analysis Date = 12/12/11 Pct Recovery = 73% Analysis Date = 12/12/11 Pct Recovery = 73% Analysis Date = 12/02/11 Pct Recovery = 73% Analysis Date = 12/02/11 Pct Recovery = 73% Analysis Date = 11/21/11 Pct Recovery = 72% Analysis Date = 11/21/11 Pct Recovery = 72% Analysis Date = 11/10/11 Pct Recovery = 72% Analysis Date = 11/10/11 Pct Recovery = 72% Analysis Date = 10/30/11 Pct Recovery = 72% Analysis Date = 10/30/11 Pct Recovery = 72% Analysis Date = 10/20/11 Pct Recovery = 72% Analysis Date = 10/20/11 Pct Recovery = 72% Analysis Date = 10/09/11 Pct Recovery = 72% Analysis Date = 10/09/11 Pct Recovery = 72% Analysis Date = 09/28/11 Pct Recovery = 72% Analysis Date = 09/28/11 Pct Recovery = 72% Analysis Date = 09/18/11 Pct Recovery = 71% Analysis Date = 09/18/11 Pct Recovery = 71% Analysis Date = 09/07/11 Pct Recovery = 71% Analysis Date = 09/07/11 Pct Recovery = 71% Analysis Date = 08/27/11 Pct Recovery = 71% Analysis Date = 08/27/11 Pct Recovery = 71% Analysis Date = 08/17/11 Pct Recovery = 71% Analysis Date = 08/17/11 Pct Recovery = 71% Analysis Date = 08/06/11 Pct Recovery = 71% Analysis Date = 08/06/11 Pct Recovery = 71% Analysis Date = 07/26/11 Pct Recovery = 70% Analysis Date = 07/26/11 Pct Recovery = 70% Analysis Date = 07/16/11 Pct Recovery = 70% Analysis Date = 07/16/11 Pct Recovery = 70% Analysis Date = 07/05/11 Pct Recovery = 70% Analysis Date = 07/05/11 Pct Recovery = 70% Analysis Date = 06/24/11 Pct Recovery = 70% Analysis Date = 06/24/11 Pct Recovery = 70% Analysis Date = 06/14/11 Pct Recovery = 70% Analysis Date = 06/14/11 Pct Recovery = 70% Analysis Date = 06/03/11 Pct Recovery = 70% Analysis Date = 06/03/11 Pct Recovery = 70% Analysis Date = 05/23/11 Pct Recovery = 69% Analysis Date = 05/23/11 Pct Recovery = 69% Analysis Date = 05/13/11 Pct Recovery = 69% Analysis Date = 05/13/11 Pct Recovery = 69% Analysis Date = 05/02/11 Pct Recovery = 69% Analysis Date = 05/02/11 Pct Recovery = 69% Analysis Date = 04/21/11 Pct Recovery = 69% Analysis Date = 04/21/11 Pct Recovery = 69% Analysis Date = 04/11/11 Pct Recovery = 69% Analysis Date = 04/11/11 Pct Recovery = 69% Analysis Date = 03/31/11 Pct Recovery = 68% Analysis Date = 03/31/11 Pct Recovery = 68% Analysis Date = 03/20/11 Pct Recovery = 68% Analysis Date = 03/20/11 Pct Recovery = 68% Analysis Date = 03/10/11 Pct Recovery = 68% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
BISPHENOL A

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 71 77% 21% 73% 22%
Total 71 77% 21% 73% 22%

Sample Statistics
BISPHENOL A

Characteristic N % % Basis
Plotted 71 99% Spiked
Estimated Values 36 50% Spiked
Deleted Values 4 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 75 .  
False Negatives 1 1% 1 out of 72
Not Spiked 56 .  
False Positives 0 0% 0 out of 55

BQS OBSP Determination:
CHOLESTEROL
METHOD: 4434 , TESTIDCODE: 64534GM005
Open Data Set

Analysis Date = 12/03/12 SpikeMix = ERA 0511-12-02: 50 µl & Abs 051512: 50 µl Pct Recovery = 111% Analysis Date = 02/22/13 SpikeMix = Restek A089631: 50 µl & Supelco LB92781: 50 µl Pct Recovery = 113% Analysis Date = 12/18/12 SpikeMix = Spex Organics T1120525010: 50 µl & Supelco LB92781: 50 µl Pct Recovery = 96% Analysis Date = 05/09/11 SpikeMix = Abs 081810: 100 µl Pct Recovery = 82% Analysis Date = 07/02/12 SpikeMix = Abs 081810: 100 µl Pct Recovery = 99% Analysis Date = 04/17/12 SpikeMix = Abs 081810: 100 µl Pct Recovery = 99% Analysis Date = 10/03/11 SpikeMix = Abs 081810: 100 µl Pct Recovery = 82% Analysis Date = 02/01/12 SpikeMix = Spex Organics T1100629008: 100 µl Pct Recovery = 98% Analysis Date = 09/29/11 SpikeMix = Spex Organics T1100629008: 100 µl Pct Recovery = 83% Analysis Date = 03/31/11 SpikeMix = Spex Organics T1100629008: 100 µl Pct Recovery = 78% Analysis Date = 04/03/13 SpikeMix = Spex Organics T1120525010: 25 µl & Abs 051512: 25 µl Pct Recovery = 114% Analysis Date = 11/01/12 SpikeMix = ERA 0507-12-04.1: 25 µl & Abs 051512: 25 µl Pct Recovery = 113% Analysis Date = 08/31/12 SpikeMix = ERA 0511-12-02: 25 µl & Abs 051512: 25 µl Pct Recovery = 114% Analysis Date = 08/24/12 SpikeMix = Abs 051512: 25 µl Pct Recovery = 123% Analysis Date = 04/10/13 SpikeMix = ERA 0511-12-02: 25 µl & Supelco LB92781: 25 µl Pct Recovery = 115% Analysis Date = 02/08/13 SpikeMix = ERA 0507-12-04.1: 25 µl & Supelco LB92781: 25 µl Pct Recovery = 132% Analysis Date = 12/18/12 SpikeMix = Restek A089631: 25 µl & Supelco LB92781: 25 µl Pct Recovery = 96% Analysis Date = 03/27/12 SpikeMix = Abs 081810: 25 µl Pct Recovery = 97% Analysis Date = 01/27/12 SpikeMix = Abs 081810: 25 µl Pct Recovery = 147% Analysis Date = 10/12/11 SpikeMix = Abs 081810: 25 µl Pct Recovery = 105% Analysis Date = 05/26/11 SpikeMix = Spex Organics T1100629008: 25 µl Pct Recovery = 96% Analysis Date = 08/16/12 SpikeMix = Spex Organics T1100629008: 25 µl Pct Recovery = 129% Analysis Date = 11/28/11 SpikeMix = Spex Organics T1100629008: 25 µl Pct Recovery = 89% Analysis Date = 10/13/11 SpikeMix = Spex Organics T1100629008: 25 µl Pct Recovery = 99% Analysis Date = 06/13/11 SpikeMix = Abs 081810: 25 µl Pct Recovery = 107% Analysis Date = 03/30/11 SpikeMix = Abs 081810: 25 µl Pct Recovery = 84% Analysis Date = 03/10/11 SpikeMix = Spex Organics T1100629008: 25 µl Pct Recovery = 88% Analysis Date = 07/11/11 SpikeMix = Spex Organics T1100629008: 25 µl Pct Recovery = 86% Analysis Date = 03/14/14 SpikeMix = Supelco LB99393: 50 µl & Abs 050813: 50 µl Pct Recovery = 81% Analysis Date = 02/25/14 SpikeMix = ERA 0415-13-01.1A: 50 µl & Abs 050813: 50 µl Pct Recovery = 89% Analysis Date = 03/05/14 SpikeMix = Spex Organics T1130423008: 50 µl & Abs 071513: 50 µl Pct Recovery = 73% Analysis Date = 08/09/13 SpikeMix = ERA 0415-13-01.2A: 50 µl & Spex Organics T1130423008: 50 µl Pct Recovery = 77% Analysis Date = 08/31/16 SpikeMix = Spex Organics TS160420010: 50 µl & ChemService 5016200: 50 µl Pct Recovery = 72% Analysis Date = 12/15/16 SpikeMix = Abs 061416H: 50 µl & ChemService 5016100: 50 µl Pct Recovery = 61% Analysis Date = 04/01/15 SpikeMix = Spex Organics E1140505004: 60 µl & Supelco LC06946: 60 µl Pct Recovery = 61% Analysis Date = 02/12/15 SpikeMix = Supelco LC06946: 60 µl & Abs 042114: 60 µl Pct Recovery = 72% Analysis Date = 12/09/14 SpikeMix = Abs 031014: 60 µl & Supelco LC06946: 60 µl Pct Recovery = 74% Analysis Date = 09/23/14 SpikeMix = Supelco LC06946: 60 µl & ChemService 2561700: 60 µl Pct Recovery = 72% Analysis Date = 04/01/15 SpikeMix = ERA 0227-14-07.2: 60 µl & ChemService 2561700: 60 µl Pct Recovery = 48% Analysis Date = 08/22/14 SpikeMix = ERA 0227-14-07.2: 60 µl & Abs 042114: 60 µl Pct Recovery = 53% Analysis Date = 08/11/14 SpikeMix = Abs 031014: 60 µl & ERA 0227-14-07.2: 60 µl Pct Recovery = 72% Analysis Date = 01/05/16 SpikeMix = Supelco LC13547: 60 µl & ChemService 4073900: 60 µl Pct Recovery = 96% Analysis Date = 01/07/16 SpikeMix = Crescent 04EE007: 60 µl & Abs 041515: 60 µl Pct Recovery = 85% Analysis Date = 09/14/15 SpikeMix = ERA 0601-15-04: 50 µl & ChemService 4073900: 50 µl Pct Recovery = 93% Analysis Date = 08/17/15 SpikeMix = ChemService 4073900: 50 µl & Abs 041515: 50 µl Pct Recovery = 61% Analysis Date = 01/08/16 SpikeMix = Crescent 04EE007: 50 µl & Spex Organics EN150501025: 50 µl Pct Recovery = 72% Analysis Date = 08/10/15 SpikeMix = ERA 0601-15-04: 50 µl & Crescent 04EE007: 50 µl Pct Recovery = 82% Analysis Date = 03/03/14 SpikeMix = Abs 050813: 20 µl & Abs 071513: 20 µl Pct Recovery = 68% Analysis Date = 02/19/14 SpikeMix = Abs 050813: 20 µl & Abs 071513: 20 µl Pct Recovery = 94% Analysis Date = 11/18/13 SpikeMix = ERA 0415-13-01.2A: 20 µl & Abs 050813: 20 µl Pct Recovery = 74% Analysis Date = 12/09/13 SpikeMix = Supelco LB99393: 20 µl & Spex Organics T1130423008: 20 µl Pct Recovery = 148% Analysis Date = 06/27/13 SpikeMix = ERA 0415-13-01.1A: 20 µl & Spex Organics T1130423008: 20 µl Pct Recovery = 71% Analysis Date = 06/04/13 SpikeMix = Supelco LB99393: 20 µl & Spex Organics T1130423008: 20 µl Pct Recovery = 73% Analysis Date = 01/29/15 SpikeMix = Abs 031014: 30 µl & Supelco LC06946: 30 µl Pct Recovery = 58% Analysis Date = 01/21/15 SpikeMix = Supelco LC06946: 30 µl & ChemService 2561700: 30 µl Pct Recovery = 66% Analysis Date = 12/23/14 SpikeMix = Spex Organics E1140505004: 30 µl & Supelco LC06946: 30 µl Pct Recovery = 83% Analysis Date = 12/16/14 SpikeMix = Supelco LC06946: 30 µl & Abs 042114: 30 µl Pct Recovery = 94% Analysis Date = 06/03/15 SpikeMix = Abs 031014: 30 µl & ERA 0227-14-07.2: 30 µl Pct Recovery = 78% Analysis Date = 11/05/14 SpikeMix = ERA 0227-14-07.2: 30 µl & Abs 042114: 30 µl Pct Recovery = 54% Analysis Date = 09/04/14 SpikeMix = ERA 0227-14-07.2: 30 µl & Spex Organics E1140505004: 30 µl Pct Recovery = 77% Analysis Date = 07/28/14 SpikeMix = ERA 0227-14-07.2: 30 µl & ChemService 2561700: 30 µl Pct Recovery = 78% Analysis Date = 07/14/14 SpikeMix = ERA 0227-14-07.2: 30 µl & Abs 031014: 30 µl Pct Recovery = 66% Analysis Date = 03/18/16 SpikeMix = Supelco LC13547: 30 µl & ChemService 4073900: 30 µl Pct Recovery = 70% Analysis Date = 01/08/16 SpikeMix = ERA 0601-15-04: 30 µl & ChemService 4073900: 30 µl Pct Recovery = 70% Analysis Date = 09/23/15 SpikeMix = ChemService 4073900: 30 µl & Spex Organics EN150501025: 30 µl Pct Recovery = 88% Analysis Date = 01/08/16 SpikeMix = ERA 0601-15-04: 30 µl & Crescent 04EE007: 30 µl Pct Recovery = 93% Analysis Date = 12/11/15 SpikeMix = Crescent 04EE007: 30 µl & Spex Organics EN150501025: 30 µl Pct Recovery = 68% Analysis Date = 12/14/16 Pct Recovery = 75% Analysis Date = 12/04/16 Pct Recovery = 75% Analysis Date = 12/04/16 Pct Recovery = 75% Analysis Date = 11/23/16 Pct Recovery = 75% Analysis Date = 11/23/16 Pct Recovery = 75% Analysis Date = 11/13/16 Pct Recovery = 75% Analysis Date = 11/13/16 Pct Recovery = 75% Analysis Date = 11/02/16 Pct Recovery = 75% Analysis Date = 11/02/16 Pct Recovery = 75% Analysis Date = 10/23/16 Pct Recovery = 75% Analysis Date = 10/23/16 Pct Recovery = 75% Analysis Date = 10/12/16 Pct Recovery = 75% Analysis Date = 10/12/16 Pct Recovery = 75% Analysis Date = 10/02/16 Pct Recovery = 75% Analysis Date = 10/02/16 Pct Recovery = 75% Analysis Date = 09/21/16 Pct Recovery = 75% Analysis Date = 09/21/16 Pct Recovery = 75% Analysis Date = 09/11/16 Pct Recovery = 75% Analysis Date = 09/11/16 Pct Recovery = 75% Analysis Date = 08/31/16 Pct Recovery = 75% Analysis Date = 08/31/16 Pct Recovery = 75% Analysis Date = 08/21/16 Pct Recovery = 75% Analysis Date = 08/21/16 Pct Recovery = 75% Analysis Date = 08/10/16 Pct Recovery = 75% Analysis Date = 08/10/16 Pct Recovery = 75% Analysis Date = 07/31/16 Pct Recovery = 75% Analysis Date = 07/31/16 Pct Recovery = 75% Analysis Date = 07/20/16 Pct Recovery = 75% Analysis Date = 07/20/16 Pct Recovery = 75% Analysis Date = 07/09/16 Pct Recovery = 75% Analysis Date = 07/09/16 Pct Recovery = 75% Analysis Date = 06/29/16 Pct Recovery = 75% Analysis Date = 06/29/16 Pct Recovery = 75% Analysis Date = 06/18/16 Pct Recovery = 75% Analysis Date = 06/18/16 Pct Recovery = 75% Analysis Date = 06/08/16 Pct Recovery = 75% Analysis Date = 06/08/16 Pct Recovery = 75% Analysis Date = 05/28/16 Pct Recovery = 75% Analysis Date = 05/28/16 Pct Recovery = 75% Analysis Date = 05/18/16 Pct Recovery = 75% Analysis Date = 05/18/16 Pct Recovery = 75% Analysis Date = 05/07/16 Pct Recovery = 75% Analysis Date = 05/07/16 Pct Recovery = 75% Analysis Date = 04/27/16 Pct Recovery = 75% Analysis Date = 04/27/16 Pct Recovery = 75% Analysis Date = 04/16/16 Pct Recovery = 75% Analysis Date = 04/16/16 Pct Recovery = 75% Analysis Date = 04/06/16 Pct Recovery = 75% Analysis Date = 04/06/16 Pct Recovery = 75% Analysis Date = 03/26/16 Pct Recovery = 75% Analysis Date = 03/26/16 Pct Recovery = 75% Analysis Date = 03/16/16 Pct Recovery = 75% Analysis Date = 03/16/16 Pct Recovery = 75% Analysis Date = 03/05/16 Pct Recovery = 75% Analysis Date = 03/05/16 Pct Recovery = 75% Analysis Date = 02/24/16 Pct Recovery = 75% Analysis Date = 02/24/16 Pct Recovery = 75% Analysis Date = 02/13/16 Pct Recovery = 75% Analysis Date = 02/13/16 Pct Recovery = 75% Analysis Date = 02/02/16 Pct Recovery = 75% Analysis Date = 02/02/16 Pct Recovery = 75% Analysis Date = 01/23/16 Pct Recovery = 75% Analysis Date = 01/23/16 Pct Recovery = 75% Analysis Date = 01/12/16 Pct Recovery = 75% Analysis Date = 01/12/16 Pct Recovery = 75% Analysis Date = 01/02/16 Pct Recovery = 74% Analysis Date = 01/02/16 Pct Recovery = 74% Analysis Date = 12/22/15 Pct Recovery = 74% Analysis Date = 12/22/15 Pct Recovery = 74% Analysis Date = 12/12/15 Pct Recovery = 74% Analysis Date = 12/12/15 Pct Recovery = 74% Analysis Date = 12/01/15 Pct Recovery = 74% Analysis Date = 12/01/15 Pct Recovery = 74% Analysis Date = 11/21/15 Pct Recovery = 74% Analysis Date = 11/21/15 Pct Recovery = 74% Analysis Date = 11/10/15 Pct Recovery = 75% Analysis Date = 11/10/15 Pct Recovery = 75% Analysis Date = 10/31/15 Pct Recovery = 75% Analysis Date = 10/31/15 Pct Recovery = 75% Analysis Date = 10/20/15 Pct Recovery = 75% Analysis Date = 10/20/15 Pct Recovery = 75% Analysis Date = 10/10/15 Pct Recovery = 75% Analysis Date = 10/10/15 Pct Recovery = 75% Analysis Date = 09/29/15 Pct Recovery = 75% Analysis Date = 09/29/15 Pct Recovery = 75% Analysis Date = 09/18/15 Pct Recovery = 75% Analysis Date = 09/18/15 Pct Recovery = 75% Analysis Date = 09/08/15 Pct Recovery = 75% Analysis Date = 09/08/15 Pct Recovery = 75% Analysis Date = 08/28/15 Pct Recovery = 75% Analysis Date = 08/28/15 Pct Recovery = 75% Analysis Date = 08/18/15 Pct Recovery = 75% Analysis Date = 08/18/15 Pct Recovery = 75% Analysis Date = 08/07/15 Pct Recovery = 75% Analysis Date = 08/07/15 Pct Recovery = 75% Analysis Date = 07/28/15 Pct Recovery = 75% Analysis Date = 07/28/15 Pct Recovery = 75% Analysis Date = 07/17/15 Pct Recovery = 75% Analysis Date = 07/17/15 Pct Recovery = 75% Analysis Date = 07/07/15 Pct Recovery = 75% Analysis Date = 07/07/15 Pct Recovery = 75% Analysis Date = 06/26/15 Pct Recovery = 75% Analysis Date = 06/26/15 Pct Recovery = 75% Analysis Date = 06/16/15 Pct Recovery = 75% Analysis Date = 06/16/15 Pct Recovery = 75% Analysis Date = 06/05/15 Pct Recovery = 75% Analysis Date = 06/05/15 Pct Recovery = 75% Analysis Date = 05/26/15 Pct Recovery = 75% Analysis Date = 05/26/15 Pct Recovery = 75% Analysis Date = 05/15/15 Pct Recovery = 75% Analysis Date = 05/15/15 Pct Recovery = 75% Analysis Date = 05/05/15 Pct Recovery = 75% Analysis Date = 05/05/15 Pct Recovery = 75% Analysis Date = 04/24/15 Pct Recovery = 75% Analysis Date = 04/24/15 Pct Recovery = 75% Analysis Date = 04/13/15 Pct Recovery = 75% Analysis Date = 04/13/15 Pct Recovery = 75% Analysis Date = 04/03/15 Pct Recovery = 75% Analysis Date = 04/03/15 Pct Recovery = 75% Analysis Date = 03/23/15 Pct Recovery = 75% Analysis Date = 03/23/15 Pct Recovery = 75% Analysis Date = 03/13/15 Pct Recovery = 75% Analysis Date = 03/13/15 Pct Recovery = 75% Analysis Date = 03/02/15 Pct Recovery = 75% Analysis Date = 03/02/15 Pct Recovery = 75% Analysis Date = 02/20/15 Pct Recovery = 75% Analysis Date = 02/20/15 Pct Recovery = 75% Analysis Date = 02/09/15 Pct Recovery = 75% Analysis Date = 02/09/15 Pct Recovery = 75% Analysis Date = 01/30/15 Pct Recovery = 75% Analysis Date = 01/30/15 Pct Recovery = 75% Analysis Date = 01/19/15 Pct Recovery = 75% Analysis Date = 01/19/15 Pct Recovery = 75% Analysis Date = 01/09/15 Pct Recovery = 75% Analysis Date = 01/09/15 Pct Recovery = 75% Analysis Date = 12/29/14 Pct Recovery = 75% Analysis Date = 12/29/14 Pct Recovery = 75% Analysis Date = 12/19/14 Pct Recovery = 75% Analysis Date = 12/19/14 Pct Recovery = 75% Analysis Date = 12/08/14 Pct Recovery = 75% Analysis Date = 12/08/14 Pct Recovery = 75% Analysis Date = 11/28/14 Pct Recovery = 75% Analysis Date = 11/28/14 Pct Recovery = 75% Analysis Date = 11/17/14 Pct Recovery = 75% Analysis Date = 11/17/14 Pct Recovery = 75% Analysis Date = 11/06/14 Pct Recovery = 75% Analysis Date = 11/06/14 Pct Recovery = 75% Analysis Date = 10/27/14 Pct Recovery = 75% Analysis Date = 10/27/14 Pct Recovery = 75% Analysis Date = 10/16/14 Pct Recovery = 75% Analysis Date = 10/16/14 Pct Recovery = 75% Analysis Date = 10/06/14 Pct Recovery = 75% Analysis Date = 10/06/14 Pct Recovery = 75% Analysis Date = 09/25/14 Pct Recovery = 75% Analysis Date = 09/25/14 Pct Recovery = 75% Analysis Date = 09/15/14 Pct Recovery = 76% Analysis Date = 09/15/14 Pct Recovery = 76% Analysis Date = 09/04/14 Pct Recovery = 76% Analysis Date = 09/04/14 Pct Recovery = 76% Analysis Date = 08/25/14 Pct Recovery = 76% Analysis Date = 08/25/14 Pct Recovery = 76% Analysis Date = 08/14/14 Pct Recovery = 76% Analysis Date = 08/14/14 Pct Recovery = 76% Analysis Date = 08/04/14 Pct Recovery = 76% Analysis Date = 08/04/14 Pct Recovery = 76% Analysis Date = 07/24/14 Pct Recovery = 77% Analysis Date = 07/24/14 Pct Recovery = 77% Analysis Date = 07/14/14 Pct Recovery = 77% Analysis Date = 07/14/14 Pct Recovery = 77% Analysis Date = 07/03/14 Pct Recovery = 77% Analysis Date = 07/03/14 Pct Recovery = 77% Analysis Date = 06/22/14 Pct Recovery = 78% Analysis Date = 06/22/14 Pct Recovery = 78% Analysis Date = 06/12/14 Pct Recovery = 78% Analysis Date = 06/12/14 Pct Recovery = 78% Analysis Date = 06/01/14 Pct Recovery = 79% Analysis Date = 06/01/14 Pct Recovery = 79% Analysis Date = 05/22/14 Pct Recovery = 79% Analysis Date = 05/22/14 Pct Recovery = 79% Analysis Date = 05/11/14 Pct Recovery = 80% Analysis Date = 05/11/14 Pct Recovery = 80% Analysis Date = 05/01/14 Pct Recovery = 80% Analysis Date = 05/01/14 Pct Recovery = 80% Analysis Date = 04/20/14 Pct Recovery = 81% Analysis Date = 04/20/14 Pct Recovery = 81% Analysis Date = 04/10/14 Pct Recovery = 81% Analysis Date = 04/10/14 Pct Recovery = 81% Analysis Date = 03/30/14 Pct Recovery = 82% Analysis Date = 03/30/14 Pct Recovery = 82% Analysis Date = 03/20/14 Pct Recovery = 82% Analysis Date = 03/20/14 Pct Recovery = 82% Analysis Date = 03/09/14 Pct Recovery = 83% Analysis Date = 03/09/14 Pct Recovery = 83% Analysis Date = 02/27/14 Pct Recovery = 83% Analysis Date = 02/27/14 Pct Recovery = 83% Analysis Date = 02/16/14 Pct Recovery = 84% Analysis Date = 02/16/14 Pct Recovery = 84% Analysis Date = 02/06/14 Pct Recovery = 84% Analysis Date = 02/06/14 Pct Recovery = 84% Analysis Date = 01/26/14 Pct Recovery = 85% Analysis Date = 01/26/14 Pct Recovery = 85% Analysis Date = 01/15/14 Pct Recovery = 85% Analysis Date = 01/15/14 Pct Recovery = 85% Analysis Date = 01/05/14 Pct Recovery = 86% Analysis Date = 01/05/14 Pct Recovery = 86% Analysis Date = 12/25/13 Pct Recovery = 86% Analysis Date = 12/25/13 Pct Recovery = 86% Analysis Date = 12/15/13 Pct Recovery = 87% Analysis Date = 12/15/13 Pct Recovery = 87% Analysis Date = 12/04/13 Pct Recovery = 87% Analysis Date = 12/04/13 Pct Recovery = 87% Analysis Date = 11/24/13 Pct Recovery = 88% Analysis Date = 11/24/13 Pct Recovery = 88% Analysis Date = 11/13/13 Pct Recovery = 89% Analysis Date = 11/13/13 Pct Recovery = 89% Analysis Date = 11/03/13 Pct Recovery = 89% Analysis Date = 11/03/13 Pct Recovery = 89% Analysis Date = 10/23/13 Pct Recovery = 90% Analysis Date = 10/23/13 Pct Recovery = 90% Analysis Date = 10/13/13 Pct Recovery = 90% Analysis Date = 10/13/13 Pct Recovery = 90% Analysis Date = 10/02/13 Pct Recovery = 91% Analysis Date = 10/02/13 Pct Recovery = 91% Analysis Date = 09/22/13 Pct Recovery = 91% Analysis Date = 09/22/13 Pct Recovery = 91% Analysis Date = 09/11/13 Pct Recovery = 92% Analysis Date = 09/11/13 Pct Recovery = 92% Analysis Date = 09/01/13 Pct Recovery = 92% Analysis Date = 09/01/13 Pct Recovery = 92% Analysis Date = 08/21/13 Pct Recovery = 93% Analysis Date = 08/21/13 Pct Recovery = 93% Analysis Date = 08/10/13 Pct Recovery = 93% Analysis Date = 08/10/13 Pct Recovery = 93% Analysis Date = 07/31/13 Pct Recovery = 94% Analysis Date = 07/31/13 Pct Recovery = 94% Analysis Date = 07/20/13 Pct Recovery = 94% Analysis Date = 07/20/13 Pct Recovery = 94% Analysis Date = 07/10/13 Pct Recovery = 95% Analysis Date = 07/10/13 Pct Recovery = 95% Analysis Date = 06/29/13 Pct Recovery = 95% Analysis Date = 06/29/13 Pct Recovery = 95% Analysis Date = 06/19/13 Pct Recovery = 96% Analysis Date = 06/19/13 Pct Recovery = 96% Analysis Date = 06/08/13 Pct Recovery = 96% Analysis Date = 06/08/13 Pct Recovery = 96% Analysis Date = 05/29/13 Pct Recovery = 97% Analysis Date = 05/29/13 Pct Recovery = 97% Analysis Date = 05/18/13 Pct Recovery = 98% Analysis Date = 05/18/13 Pct Recovery = 98% Analysis Date = 05/08/13 Pct Recovery = 98% Analysis Date = 05/08/13 Pct Recovery = 98% Analysis Date = 04/27/13 Pct Recovery = 99% Analysis Date = 04/27/13 Pct Recovery = 99% Analysis Date = 04/17/13 Pct Recovery = 99% Analysis Date = 04/17/13 Pct Recovery = 99% Analysis Date = 04/06/13 Pct Recovery = 100% Analysis Date = 04/06/13 Pct Recovery = 100% Analysis Date = 03/26/13 Pct Recovery = 100% Analysis Date = 03/26/13 Pct Recovery = 100% Analysis Date = 03/16/13 Pct Recovery = 101% Analysis Date = 03/16/13 Pct Recovery = 101% Analysis Date = 03/05/13 Pct Recovery = 101% Analysis Date = 03/05/13 Pct Recovery = 101% Analysis Date = 02/23/13 Pct Recovery = 102% Analysis Date = 02/23/13 Pct Recovery = 102% Analysis Date = 02/12/13 Pct Recovery = 102% Analysis Date = 02/12/13 Pct Recovery = 102% Analysis Date = 02/02/13 Pct Recovery = 102% Analysis Date = 02/02/13 Pct Recovery = 102% Analysis Date = 01/22/13 Pct Recovery = 103% Analysis Date = 01/22/13 Pct Recovery = 103% Analysis Date = 01/12/13 Pct Recovery = 103% Analysis Date = 01/12/13 Pct Recovery = 103% Analysis Date = 01/01/13 Pct Recovery = 103% Analysis Date = 01/01/13 Pct Recovery = 103% Analysis Date = 12/22/12 Pct Recovery = 103% Analysis Date = 12/22/12 Pct Recovery = 103% Analysis Date = 12/11/12 Pct Recovery = 103% Analysis Date = 12/11/12 Pct Recovery = 103% Analysis Date = 12/01/12 Pct Recovery = 104% Analysis Date = 12/01/12 Pct Recovery = 104% Analysis Date = 11/20/12 Pct Recovery = 104% Analysis Date = 11/20/12 Pct Recovery = 104% Analysis Date = 11/10/12 Pct Recovery = 103% Analysis Date = 11/10/12 Pct Recovery = 103% Analysis Date = 10/30/12 Pct Recovery = 103% Analysis Date = 10/30/12 Pct Recovery = 103% Analysis Date = 10/19/12 Pct Recovery = 103% Analysis Date = 10/19/12 Pct Recovery = 103% Analysis Date = 10/09/12 Pct Recovery = 103% Analysis Date = 10/09/12 Pct Recovery = 103% Analysis Date = 09/28/12 Pct Recovery = 103% Analysis Date = 09/28/12 Pct Recovery = 103% Analysis Date = 09/18/12 Pct Recovery = 103% Analysis Date = 09/18/12 Pct Recovery = 103% Analysis Date = 09/07/12 Pct Recovery = 103% Analysis Date = 09/07/12 Pct Recovery = 103% Analysis Date = 08/28/12 Pct Recovery = 103% Analysis Date = 08/28/12 Pct Recovery = 103% Analysis Date = 08/17/12 Pct Recovery = 102% Analysis Date = 08/17/12 Pct Recovery = 102% Analysis Date = 08/07/12 Pct Recovery = 102% Analysis Date = 08/07/12 Pct Recovery = 102% Analysis Date = 07/27/12 Pct Recovery = 102% Analysis Date = 07/27/12 Pct Recovery = 102% Analysis Date = 07/17/12 Pct Recovery = 102% Analysis Date = 07/17/12 Pct Recovery = 102% Analysis Date = 07/06/12 Pct Recovery = 102% Analysis Date = 07/06/12 Pct Recovery = 102% Analysis Date = 06/26/12 Pct Recovery = 102% Analysis Date = 06/26/12 Pct Recovery = 102% Analysis Date = 06/15/12 Pct Recovery = 102% Analysis Date = 06/15/12 Pct Recovery = 102% Analysis Date = 06/05/12 Pct Recovery = 101% Analysis Date = 06/05/12 Pct Recovery = 101% Analysis Date = 05/25/12 Pct Recovery = 101% Analysis Date = 05/25/12 Pct Recovery = 101% Analysis Date = 05/14/12 Pct Recovery = 101% Analysis Date = 05/14/12 Pct Recovery = 101% Analysis Date = 05/04/12 Pct Recovery = 101% Analysis Date = 05/04/12 Pct Recovery = 101% Analysis Date = 04/23/12 Pct Recovery = 101% Analysis Date = 04/23/12 Pct Recovery = 101% Analysis Date = 04/13/12 Pct Recovery = 100% Analysis Date = 04/13/12 Pct Recovery = 100% Analysis Date = 04/02/12 Pct Recovery = 100% Analysis Date = 04/02/12 Pct Recovery = 100% Analysis Date = 03/23/12 Pct Recovery = 100% Analysis Date = 03/23/12 Pct Recovery = 100% Analysis Date = 03/12/12 Pct Recovery = 100% Analysis Date = 03/12/12 Pct Recovery = 100% Analysis Date = 03/02/12 Pct Recovery = 99% Analysis Date = 03/02/12 Pct Recovery = 99% Analysis Date = 02/20/12 Pct Recovery = 99% Analysis Date = 02/20/12 Pct Recovery = 99% Analysis Date = 02/10/12 Pct Recovery = 99% Analysis Date = 02/10/12 Pct Recovery = 99% Analysis Date = 01/30/12 Pct Recovery = 99% Analysis Date = 01/30/12 Pct Recovery = 99% Analysis Date = 01/20/12 Pct Recovery = 99% Analysis Date = 01/20/12 Pct Recovery = 99% Analysis Date = 01/09/12 Pct Recovery = 98% Analysis Date = 01/09/12 Pct Recovery = 98% Analysis Date = 12/29/11 Pct Recovery = 98% Analysis Date = 12/29/11 Pct Recovery = 98% Analysis Date = 12/19/11 Pct Recovery = 98% Analysis Date = 12/19/11 Pct Recovery = 98% Analysis Date = 12/08/11 Pct Recovery = 98% Analysis Date = 12/08/11 Pct Recovery = 98% Analysis Date = 11/28/11 Pct Recovery = 98% Analysis Date = 11/28/11 Pct Recovery = 98% Analysis Date = 11/17/11 Pct Recovery = 97% Analysis Date = 11/17/11 Pct Recovery = 97% Analysis Date = 11/07/11 Pct Recovery = 97% Analysis Date = 11/07/11 Pct Recovery = 97% Analysis Date = 10/27/11 Pct Recovery = 97% Analysis Date = 10/27/11 Pct Recovery = 97% Analysis Date = 10/17/11 Pct Recovery = 97% Analysis Date = 10/17/11 Pct Recovery = 97% Analysis Date = 10/06/11 Pct Recovery = 97% Analysis Date = 10/06/11 Pct Recovery = 97% Analysis Date = 09/26/11 Pct Recovery = 96% Analysis Date = 09/26/11 Pct Recovery = 96% Analysis Date = 09/15/11 Pct Recovery = 96% Analysis Date = 09/15/11 Pct Recovery = 96% Analysis Date = 09/05/11 Pct Recovery = 96% Analysis Date = 09/05/11 Pct Recovery = 96% Analysis Date = 08/25/11 Pct Recovery = 96% Analysis Date = 08/25/11 Pct Recovery = 96% Analysis Date = 08/15/11 Pct Recovery = 95% Analysis Date = 08/15/11 Pct Recovery = 95% Analysis Date = 08/04/11 Pct Recovery = 95% Analysis Date = 08/04/11 Pct Recovery = 95% Analysis Date = 07/24/11 Pct Recovery = 95% Analysis Date = 07/24/11 Pct Recovery = 95% Analysis Date = 07/14/11 Pct Recovery = 94% Analysis Date = 07/14/11 Pct Recovery = 94% Analysis Date = 07/03/11 Pct Recovery = 94% Analysis Date = 07/03/11 Pct Recovery = 94% Analysis Date = 06/23/11 Pct Recovery = 94% Analysis Date = 06/23/11 Pct Recovery = 94% Analysis Date = 06/12/11 Pct Recovery = 94% Analysis Date = 06/12/11 Pct Recovery = 94% Analysis Date = 06/02/11 Pct Recovery = 93% Analysis Date = 06/02/11 Pct Recovery = 93% Analysis Date = 05/22/11 Pct Recovery = 93% Analysis Date = 05/22/11 Pct Recovery = 93% Analysis Date = 05/12/11 Pct Recovery = 93% Analysis Date = 05/12/11 Pct Recovery = 93% Analysis Date = 05/01/11 Pct Recovery = 93% Analysis Date = 05/01/11 Pct Recovery = 93% Analysis Date = 04/21/11 Pct Recovery = 92% Analysis Date = 04/21/11 Pct Recovery = 92% Analysis Date = 04/10/11 Pct Recovery = 92% Analysis Date = 04/10/11 Pct Recovery = 92% Analysis Date = 03/31/11 Pct Recovery = 92% Analysis Date = 03/31/11 Pct Recovery = 92% Analysis Date = 03/20/11 Pct Recovery = 91% Analysis Date = 03/20/11 Pct Recovery = 91% Analysis Date = 03/10/11 Pct Recovery = 91% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
CHOLESTEROL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 67 87% 21% 83% 19%
Total 67 87% 21% 83% 19%

Sample Statistics
CHOLESTEROL

Characteristic N % % Basis
Plotted 67 87% Spiked
Estimated Values 0 0% Spiked
Deleted Values 3 2% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 80 .  
False Negatives 10 13% 10 out of 77
Not Spiked 51 .  
False Positives 2 4% 2 out of 51

BQS OBSP Determination:
CIS-ANDROSTERONE
METHOD: 4434 , TESTIDCODE: 64535GM005
Open Data Set

Analysis Date = 04/22/13 SpikeMix = ERA 0507-12-04.1: 50 µl & Restek A089631: 50 µl Pct Recovery = 76% Analysis Date = 12/18/12 SpikeMix = ERA 0507-12-04.1: 50 µl & Restek A089631: 50 µl Pct Recovery = 82% Analysis Date = 11/07/12 SpikeMix = ERA 0507-12-04.1: 50 µl & ERA 0511-12-02: 50 µl Pct Recovery = 75% Analysis Date = 03/27/12 SpikeMix = Crescent 162776: 100 µl Pct Recovery = 102% Analysis Date = 03/10/11 SpikeMix = Crescent 162776: 100 µl Pct Recovery = 72% Analysis Date = 06/23/11 SpikeMix = Crescent 162776: 100 µl Pct Recovery = 79% Analysis Date = 02/08/13 SpikeMix = ERA 0507-12-04.1: 25 µl & Supelco LB92781: 25 µl Pct Recovery = 80% Analysis Date = 11/01/12 SpikeMix = ERA 0507-12-04.1: 25 µl & Abs 051512: 25 µl Pct Recovery = 85% Analysis Date = 03/14/14 SpikeMix = Supelco LB99393: 50 µl & Abs 050813: 50 µl Pct Recovery = 76% Analysis Date = 03/14/14 SpikeMix = Supelco LB99393: 50 µl & Abs 060413: 50 µl & Abs 071513: 50 µl Pct Recovery = 47% Analysis Date = 04/14/14 SpikeMix = ERA 0415-13-01.1A: 50 µl & Abs 071513: 50 µl Pct Recovery = 67% Analysis Date = 03/05/14 SpikeMix = ERA 0415-13-01.1A: 50 µl & Abs 060413: 50 µl & Abs 071513: 50 µl Pct Recovery = 67% Analysis Date = 02/25/14 SpikeMix = ERA 0415-13-01.1A: 50 µl & Abs 050813: 50 µl Pct Recovery = 51% Analysis Date = 12/15/16 SpikeMix = Abs 061416H: 50 µl & ChemService 5016100: 50 µl Pct Recovery = 77% Analysis Date = 08/11/16 SpikeMix = ChemService 5016100: 50 µl & Spex Organics TS160420010: 50 µl Pct Recovery = 98% Analysis Date = 08/19/16 SpikeMix = Supelco LC20140V: 50 µl & Spex Organics TS160420010: 50 µl Pct Recovery = 86% Analysis Date = 04/01/15 SpikeMix = ERA 0227-14-07.2: 60 µl & ChemService 2561700: 60 µl Pct Recovery = 49% Analysis Date = 01/21/15 SpikeMix = ChemService 2561700: 60 µl & Spex Organics E1140505004: 60 µl Pct Recovery = 54% Analysis Date = 09/23/14 SpikeMix = Supelco LC06946: 60 µl & ChemService 2561700: 60 µl Pct Recovery = 81% Analysis Date = 05/06/14 SpikeMix = Abs 031014: 60 µl & ChemService 2561700: 60 µl Pct Recovery = 111% Analysis Date = 04/13/15 SpikeMix = Abs 042114: 60 µl & Spex Organics E1140505004: 60 µl Pct Recovery = 84% Analysis Date = 02/12/15 SpikeMix = Supelco LC06946: 60 µl & Abs 042114: 60 µl Pct Recovery = 59% Analysis Date = 08/26/14 SpikeMix = Abs 031014: 60 µl & Abs 042114: 60 µl Pct Recovery = 91% Analysis Date = 08/22/14 SpikeMix = ERA 0227-14-07.2: 60 µl & Abs 042114: 60 µl Pct Recovery = 65% Analysis Date = 01/05/16 SpikeMix = Supelco LC13547: 60 µl & ChemService 4073900: 60 µl Pct Recovery = 85% Analysis Date = 04/06/12 SpikeMix = Crescent 162776: 25 µl Pct Recovery = 114% Analysis Date = 11/17/11 SpikeMix = Crescent 162776: 25 µl Pct Recovery = 80% Analysis Date = 10/12/11 SpikeMix = Crescent 162776: 25 µl Pct Recovery = 95% Analysis Date = 07/25/11 SpikeMix = Crescent 162776: 25 µl Pct Recovery = 71% Analysis Date = 05/09/11 SpikeMix = Crescent 162776: 25 µl Pct Recovery = 79% Analysis Date = 03/07/16 SpikeMix = Abs 041515: 50 µl & ERA 0601-15-04: 50 µl Pct Recovery = 103% Analysis Date = 12/10/15 SpikeMix = Abs 041515: 50 µl & ERA 0601-15-04: 50 µl Pct Recovery = 85% Analysis Date = 09/14/15 SpikeMix = ERA 0601-15-04: 50 µl & ChemService 4073900: 50 µl Pct Recovery = 75% Analysis Date = 08/10/15 SpikeMix = ERA 0601-15-04: 50 µl & Crescent 04EE007: 50 µl Pct Recovery = 80% Analysis Date = 01/23/14 SpikeMix = Supelco LB99393: 20 µl & ERA 0415-13-01.2A: 20 µl & Abs 060413: 20 µl Pct Recovery = 53% Analysis Date = 12/09/13 SpikeMix = Supelco LB99393: 20 µl & Spex Organics T1130423008: 20 µl Pct Recovery = 61% Analysis Date = 07/19/13 SpikeMix = Supelco LB99393: 20 µl & ERA 0415-13-01.2A: 20 µl Pct Recovery = 43% Analysis Date = 06/04/13 SpikeMix = Supelco LB99393: 20 µl & Spex Organics T1130423008: 20 µl Pct Recovery = 68% Analysis Date = 12/29/16 SpikeMix = ChemService 5016100: 30 µl & Abs 052616: 30 µl Pct Recovery = 109% Analysis Date = 04/14/14 SpikeMix = ERA 0415-13-01.1A: 20 µl & ERA 0415-13-01.2A: 20 µl & Abs 060413: 20 µl Pct Recovery = 51% Analysis Date = 09/16/13 SpikeMix = ERA 0415-13-01.1A: 20 µl & ERA 0415-13-01.2A: 20 µl & Abs 060413: 20 µl Pct Recovery = 59% Analysis Date = 06/27/13 SpikeMix = ERA 0415-13-01.1A: 20 µl & Spex Organics T1130423008: 20 µl Pct Recovery = 60% Analysis Date = 04/01/15 SpikeMix = ChemService 2561700: 30 µl & Spex Organics E1140505004: 30 µl Pct Recovery = 88% Analysis Date = 01/21/15 SpikeMix = Supelco LC06946: 30 µl & ChemService 2561700: 30 µl Pct Recovery = 58% Analysis Date = 07/28/14 SpikeMix = ERA 0227-14-07.2: 30 µl & ChemService 2561700: 30 µl Pct Recovery = 86% Analysis Date = 05/14/14 SpikeMix = Abs 031014: 30 µl & ChemService 2561700: 30 µl Pct Recovery = 95% Analysis Date = 12/22/14 SpikeMix = Abs 042114: 30 µl & Abs 031014: 30 µl Pct Recovery = 68% Analysis Date = 12/16/14 SpikeMix = Supelco LC06946: 30 µl & Abs 042114: 30 µl Pct Recovery = 71% Analysis Date = 11/05/14 SpikeMix = ERA 0227-14-07.2: 30 µl & Abs 042114: 30 µl Pct Recovery = 80% Analysis Date = 01/08/16 SpikeMix = ERA 0601-15-04: 30 µl & ChemService 4073900: 30 µl Pct Recovery = 53% Analysis Date = 02/01/17 SpikeMix = Supelco LC20140V: 30 µl & Abs 052616: 30 µl Pct Recovery = 72% Analysis Date = 02/01/17 Pct Recovery = 91% Analysis Date = 01/21/17 Pct Recovery = 90% Analysis Date = 01/21/17 Pct Recovery = 90% Analysis Date = 01/10/17 Pct Recovery = 90% Analysis Date = 01/10/17 Pct Recovery = 90% Analysis Date = 12/30/16 Pct Recovery = 90% Analysis Date = 12/30/16 Pct Recovery = 90% Analysis Date = 12/19/16 Pct Recovery = 90% Analysis Date = 12/19/16 Pct Recovery = 90% Analysis Date = 12/09/16 Pct Recovery = 89% Analysis Date = 12/09/16 Pct Recovery = 89% Analysis Date = 11/28/16 Pct Recovery = 89% Analysis Date = 11/28/16 Pct Recovery = 89% Analysis Date = 11/17/16 Pct Recovery = 89% Analysis Date = 11/17/16 Pct Recovery = 89% Analysis Date = 11/06/16 Pct Recovery = 88% Analysis Date = 11/06/16 Pct Recovery = 88% Analysis Date = 10/27/16 Pct Recovery = 88% Analysis Date = 10/27/16 Pct Recovery = 88% Analysis Date = 10/16/16 Pct Recovery = 88% Analysis Date = 10/16/16 Pct Recovery = 88% Analysis Date = 10/05/16 Pct Recovery = 88% Analysis Date = 10/05/16 Pct Recovery = 88% Analysis Date = 09/24/16 Pct Recovery = 87% Analysis Date = 09/24/16 Pct Recovery = 87% Analysis Date = 09/13/16 Pct Recovery = 87% Analysis Date = 09/13/16 Pct Recovery = 87% Analysis Date = 09/03/16 Pct Recovery = 87% Analysis Date = 09/03/16 Pct Recovery = 87% Analysis Date = 08/23/16 Pct Recovery = 86% Analysis Date = 08/23/16 Pct Recovery = 86% Analysis Date = 08/12/16 Pct Recovery = 86% Analysis Date = 08/12/16 Pct Recovery = 86% Analysis Date = 08/01/16 Pct Recovery = 86% Analysis Date = 08/01/16 Pct Recovery = 86% Analysis Date = 07/22/16 Pct Recovery = 86% Analysis Date = 07/22/16 Pct Recovery = 86% Analysis Date = 07/11/16 Pct Recovery = 85% Analysis Date = 07/11/16 Pct Recovery = 85% Analysis Date = 06/30/16 Pct Recovery = 85% Analysis Date = 06/30/16 Pct Recovery = 85% Analysis Date = 06/19/16 Pct Recovery = 85% Analysis Date = 06/19/16 Pct Recovery = 85% Analysis Date = 06/08/16 Pct Recovery = 84% Analysis Date = 06/08/16 Pct Recovery = 84% Analysis Date = 05/29/16 Pct Recovery = 84% Analysis Date = 05/29/16 Pct Recovery = 84% Analysis Date = 05/18/16 Pct Recovery = 84% Analysis Date = 05/18/16 Pct Recovery = 84% Analysis Date = 05/07/16 Pct Recovery = 84% Analysis Date = 05/07/16 Pct Recovery = 84% Analysis Date = 04/26/16 Pct Recovery = 83% Analysis Date = 04/26/16 Pct Recovery = 83% Analysis Date = 04/16/16 Pct Recovery = 83% Analysis Date = 04/16/16 Pct Recovery = 83% Analysis Date = 04/05/16 Pct Recovery = 83% Analysis Date = 04/05/16 Pct Recovery = 83% Analysis Date = 03/25/16 Pct Recovery = 83% Analysis Date = 03/25/16 Pct Recovery = 83% Analysis Date = 03/14/16 Pct Recovery = 82% Analysis Date = 03/14/16 Pct Recovery = 82% Analysis Date = 03/03/16 Pct Recovery = 82% Analysis Date = 03/03/16 Pct Recovery = 82% Analysis Date = 02/22/16 Pct Recovery = 82% Analysis Date = 02/22/16 Pct Recovery = 82% Analysis Date = 02/11/16 Pct Recovery = 81% Analysis Date = 02/11/16 Pct Recovery = 81% Analysis Date = 01/31/16 Pct Recovery = 81% Analysis Date = 01/31/16 Pct Recovery = 81% Analysis Date = 01/20/16 Pct Recovery = 81% Analysis Date = 01/20/16 Pct Recovery = 81% Analysis Date = 01/10/16 Pct Recovery = 81% Analysis Date = 01/10/16 Pct Recovery = 81% Analysis Date = 12/30/15 Pct Recovery = 80% Analysis Date = 12/30/15 Pct Recovery = 80% Analysis Date = 12/19/15 Pct Recovery = 80% Analysis Date = 12/19/15 Pct Recovery = 80% Analysis Date = 12/08/15 Pct Recovery = 80% Analysis Date = 12/08/15 Pct Recovery = 80% Analysis Date = 11/28/15 Pct Recovery = 79% Analysis Date = 11/28/15 Pct Recovery = 79% Analysis Date = 11/17/15 Pct Recovery = 79% Analysis Date = 11/17/15 Pct Recovery = 79% Analysis Date = 11/06/15 Pct Recovery = 79% Analysis Date = 11/06/15 Pct Recovery = 79% Analysis Date = 10/26/15 Pct Recovery = 79% Analysis Date = 10/26/15 Pct Recovery = 79% Analysis Date = 10/15/15 Pct Recovery = 78% Analysis Date = 10/15/15 Pct Recovery = 78% Analysis Date = 10/05/15 Pct Recovery = 78% Analysis Date = 10/05/15 Pct Recovery = 78% Analysis Date = 09/24/15 Pct Recovery = 78% Analysis Date = 09/24/15 Pct Recovery = 78% Analysis Date = 09/13/15 Pct Recovery = 78% Analysis Date = 09/13/15 Pct Recovery = 78% Analysis Date = 09/02/15 Pct Recovery = 77% Analysis Date = 09/02/15 Pct Recovery = 77% Analysis Date = 08/23/15 Pct Recovery = 77% Analysis Date = 08/23/15 Pct Recovery = 77% Analysis Date = 08/12/15 Pct Recovery = 77% Analysis Date = 08/12/15 Pct Recovery = 77% Analysis Date = 08/01/15 Pct Recovery = 76% Analysis Date = 08/01/15 Pct Recovery = 76% Analysis Date = 07/21/15 Pct Recovery = 76% Analysis Date = 07/21/15 Pct Recovery = 76% Analysis Date = 07/10/15 Pct Recovery = 76% Analysis Date = 07/10/15 Pct Recovery = 76% Analysis Date = 06/30/15 Pct Recovery = 76% Analysis Date = 06/30/15 Pct Recovery = 76% Analysis Date = 06/19/15 Pct Recovery = 75% Analysis Date = 06/19/15 Pct Recovery = 75% Analysis Date = 06/08/15 Pct Recovery = 75% Analysis Date = 06/08/15 Pct Recovery = 75% Analysis Date = 05/28/15 Pct Recovery = 75% Analysis Date = 05/28/15 Pct Recovery = 75% Analysis Date = 05/18/15 Pct Recovery = 75% Analysis Date = 05/18/15 Pct Recovery = 75% Analysis Date = 05/07/15 Pct Recovery = 74% Analysis Date = 05/07/15 Pct Recovery = 74% Analysis Date = 04/26/15 Pct Recovery = 74% Analysis Date = 04/26/15 Pct Recovery = 74% Analysis Date = 04/15/15 Pct Recovery = 74% Analysis Date = 04/15/15 Pct Recovery = 74% Analysis Date = 04/04/15 Pct Recovery = 74% Analysis Date = 04/04/15 Pct Recovery = 74% Analysis Date = 03/25/15 Pct Recovery = 73% Analysis Date = 03/25/15 Pct Recovery = 73% Analysis Date = 03/14/15 Pct Recovery = 73% Analysis Date = 03/14/15 Pct Recovery = 73% Analysis Date = 03/03/15 Pct Recovery = 73% Analysis Date = 03/03/15 Pct Recovery = 73% Analysis Date = 02/20/15 Pct Recovery = 73% Analysis Date = 02/20/15 Pct Recovery = 73% Analysis Date = 02/10/15 Pct Recovery = 73% Analysis Date = 02/10/15 Pct Recovery = 73% Analysis Date = 01/30/15 Pct Recovery = 73% Analysis Date = 01/30/15 Pct Recovery = 73% Analysis Date = 01/19/15 Pct Recovery = 73% Analysis Date = 01/19/15 Pct Recovery = 73% Analysis Date = 01/08/15 Pct Recovery = 72% Analysis Date = 01/08/15 Pct Recovery = 72% Analysis Date = 12/28/14 Pct Recovery = 72% Analysis Date = 12/28/14 Pct Recovery = 72% Analysis Date = 12/18/14 Pct Recovery = 72% Analysis Date = 12/18/14 Pct Recovery = 72% Analysis Date = 12/07/14 Pct Recovery = 72% Analysis Date = 12/07/14 Pct Recovery = 72% Analysis Date = 11/26/14 Pct Recovery = 72% Analysis Date = 11/26/14 Pct Recovery = 72% Analysis Date = 11/15/14 Pct Recovery = 72% Analysis Date = 11/15/14 Pct Recovery = 72% Analysis Date = 11/05/14 Pct Recovery = 72% Analysis Date = 11/05/14 Pct Recovery = 72% Analysis Date = 10/25/14 Pct Recovery = 72% Analysis Date = 10/25/14 Pct Recovery = 72% Analysis Date = 10/14/14 Pct Recovery = 71% Analysis Date = 10/14/14 Pct Recovery = 71% Analysis Date = 10/03/14 Pct Recovery = 71% Analysis Date = 10/03/14 Pct Recovery = 71% Analysis Date = 09/23/14 Pct Recovery = 71% Analysis Date = 09/23/14 Pct Recovery = 71% Analysis Date = 09/12/14 Pct Recovery = 71% Analysis Date = 09/12/14 Pct Recovery = 71% Analysis Date = 09/01/14 Pct Recovery = 71% Analysis Date = 09/01/14 Pct Recovery = 71% Analysis Date = 08/21/14 Pct Recovery = 71% Analysis Date = 08/21/14 Pct Recovery = 71% Analysis Date = 08/10/14 Pct Recovery = 71% Analysis Date = 08/10/14 Pct Recovery = 71% Analysis Date = 07/31/14 Pct Recovery = 70% Analysis Date = 07/31/14 Pct Recovery = 70% Analysis Date = 07/20/14 Pct Recovery = 70% Analysis Date = 07/20/14 Pct Recovery = 70% Analysis Date = 07/09/14 Pct Recovery = 70% Analysis Date = 07/09/14 Pct Recovery = 70% Analysis Date = 06/28/14 Pct Recovery = 70% Analysis Date = 06/28/14 Pct Recovery = 70% Analysis Date = 06/18/14 Pct Recovery = 70% Analysis Date = 06/18/14 Pct Recovery = 70% Analysis Date = 06/07/14 Pct Recovery = 69% Analysis Date = 06/07/14 Pct Recovery = 69% Analysis Date = 05/27/14 Pct Recovery = 69% Analysis Date = 05/27/14 Pct Recovery = 69% Analysis Date = 05/16/14 Pct Recovery = 69% Analysis Date = 05/16/14 Pct Recovery = 69% Analysis Date = 05/05/14 Pct Recovery = 69% Analysis Date = 05/05/14 Pct Recovery = 69% Analysis Date = 04/25/14 Pct Recovery = 69% Analysis Date = 04/25/14 Pct Recovery = 69% Analysis Date = 04/14/14 Pct Recovery = 68% Analysis Date = 04/14/14 Pct Recovery = 68% Analysis Date = 04/03/14 Pct Recovery = 68% Analysis Date = 04/03/14 Pct Recovery = 68% Analysis Date = 03/23/14 Pct Recovery = 68% Analysis Date = 03/23/14 Pct Recovery = 68% Analysis Date = 03/13/14 Pct Recovery = 68% Analysis Date = 03/13/14 Pct Recovery = 68% Analysis Date = 03/02/14 Pct Recovery = 68% Analysis Date = 03/02/14 Pct Recovery = 68% Analysis Date = 02/19/14 Pct Recovery = 67% Analysis Date = 02/19/14 Pct Recovery = 67% Analysis Date = 02/08/14 Pct Recovery = 68% Analysis Date = 02/08/14 Pct Recovery = 68% Analysis Date = 01/28/14 Pct Recovery = 68% Analysis Date = 01/28/14 Pct Recovery = 68% Analysis Date = 01/18/14 Pct Recovery = 68% Analysis Date = 01/18/14 Pct Recovery = 68% Analysis Date = 01/07/14 Pct Recovery = 68% Analysis Date = 01/07/14 Pct Recovery = 68% Analysis Date = 12/27/13 Pct Recovery = 68% Analysis Date = 12/27/13 Pct Recovery = 68% Analysis Date = 12/16/13 Pct Recovery = 68% Analysis Date = 12/16/13 Pct Recovery = 68% Analysis Date = 12/06/13 Pct Recovery = 68% Analysis Date = 12/06/13 Pct Recovery = 68% Analysis Date = 11/25/13 Pct Recovery = 68% Analysis Date = 11/25/13 Pct Recovery = 68% Analysis Date = 11/14/13 Pct Recovery = 68% Analysis Date = 11/14/13 Pct Recovery = 68% Analysis Date = 11/03/13 Pct Recovery = 68% Analysis Date = 11/03/13 Pct Recovery = 68% Analysis Date = 10/23/13 Pct Recovery = 68% Analysis Date = 10/23/13 Pct Recovery = 68% Analysis Date = 10/13/13 Pct Recovery = 68% Analysis Date = 10/13/13 Pct Recovery = 68% Analysis Date = 10/02/13 Pct Recovery = 68% Analysis Date = 10/02/13 Pct Recovery = 68% Analysis Date = 09/21/13 Pct Recovery = 68% Analysis Date = 09/21/13 Pct Recovery = 68% Analysis Date = 09/10/13 Pct Recovery = 68% Analysis Date = 09/10/13 Pct Recovery = 68% Analysis Date = 08/31/13 Pct Recovery = 69% Analysis Date = 08/31/13 Pct Recovery = 69% Analysis Date = 08/20/13 Pct Recovery = 69% Analysis Date = 08/20/13 Pct Recovery = 69% Analysis Date = 08/09/13 Pct Recovery = 70% Analysis Date = 08/09/13 Pct Recovery = 70% Analysis Date = 07/29/13 Pct Recovery = 70% Analysis Date = 07/29/13 Pct Recovery = 70% Analysis Date = 07/19/13 Pct Recovery = 70% Analysis Date = 07/19/13 Pct Recovery = 70% Analysis Date = 07/08/13 Pct Recovery = 71% Analysis Date = 07/08/13 Pct Recovery = 71% Analysis Date = 06/27/13 Pct Recovery = 71% Analysis Date = 06/27/13 Pct Recovery = 71% Analysis Date = 06/16/13 Pct Recovery = 72% Analysis Date = 06/16/13 Pct Recovery = 72% Analysis Date = 06/05/13 Pct Recovery = 72% Analysis Date = 06/05/13 Pct Recovery = 72% Analysis Date = 05/26/13 Pct Recovery = 72% Analysis Date = 05/26/13 Pct Recovery = 72% Analysis Date = 05/15/13 Pct Recovery = 73% Analysis Date = 05/15/13 Pct Recovery = 73% Analysis Date = 05/04/13 Pct Recovery = 73% Analysis Date = 05/04/13 Pct Recovery = 73% Analysis Date = 04/23/13 Pct Recovery = 74% Analysis Date = 04/23/13 Pct Recovery = 74% Analysis Date = 04/13/13 Pct Recovery = 74% Analysis Date = 04/13/13 Pct Recovery = 74% Analysis Date = 04/02/13 Pct Recovery = 74% Analysis Date = 04/02/13 Pct Recovery = 74% Analysis Date = 03/22/13 Pct Recovery = 74% Analysis Date = 03/22/13 Pct Recovery = 74% Analysis Date = 03/11/13 Pct Recovery = 75% Analysis Date = 03/11/13 Pct Recovery = 75% Analysis Date = 02/28/13 Pct Recovery = 75% Analysis Date = 02/28/13 Pct Recovery = 75% Analysis Date = 02/18/13 Pct Recovery = 75% Analysis Date = 02/18/13 Pct Recovery = 75% Analysis Date = 02/07/13 Pct Recovery = 75% Analysis Date = 02/07/13 Pct Recovery = 75% Analysis Date = 01/27/13 Pct Recovery = 75% Analysis Date = 01/27/13 Pct Recovery = 75% Analysis Date = 01/16/13 Pct Recovery = 76% Analysis Date = 01/16/13 Pct Recovery = 76% Analysis Date = 01/06/13 Pct Recovery = 76% Analysis Date = 01/06/13 Pct Recovery = 76% Analysis Date = 12/26/12 Pct Recovery = 76% Analysis Date = 12/26/12 Pct Recovery = 76% Analysis Date = 12/15/12 Pct Recovery = 76% Analysis Date = 12/15/12 Pct Recovery = 76% Analysis Date = 12/04/12 Pct Recovery = 76% Analysis Date = 12/04/12 Pct Recovery = 76% Analysis Date = 11/23/12 Pct Recovery = 77% Analysis Date = 11/23/12 Pct Recovery = 77% Analysis Date = 11/13/12 Pct Recovery = 77% Analysis Date = 11/13/12 Pct Recovery = 77% Analysis Date = 11/02/12 Pct Recovery = 77% Analysis Date = 11/02/12 Pct Recovery = 77% Analysis Date = 10/22/12 Pct Recovery = 77% Analysis Date = 10/22/12 Pct Recovery = 77% Analysis Date = 10/11/12 Pct Recovery = 77% Analysis Date = 10/11/12 Pct Recovery = 77% Analysis Date = 10/01/12 Pct Recovery = 78% Analysis Date = 10/01/12 Pct Recovery = 78% Analysis Date = 09/20/12 Pct Recovery = 78% Analysis Date = 09/20/12 Pct Recovery = 78% Analysis Date = 09/09/12 Pct Recovery = 78% Analysis Date = 09/09/12 Pct Recovery = 78% Analysis Date = 08/29/12 Pct Recovery = 78% Analysis Date = 08/29/12 Pct Recovery = 78% Analysis Date = 08/18/12 Pct Recovery = 78% Analysis Date = 08/18/12 Pct Recovery = 78% Analysis Date = 08/08/12 Pct Recovery = 79% Analysis Date = 08/08/12 Pct Recovery = 79% Analysis Date = 07/28/12 Pct Recovery = 79% Analysis Date = 07/28/12 Pct Recovery = 79% Analysis Date = 07/17/12 Pct Recovery = 79% Analysis Date = 07/17/12 Pct Recovery = 79% Analysis Date = 07/06/12 Pct Recovery = 79% Analysis Date = 07/06/12 Pct Recovery = 79% Analysis Date = 06/26/12 Pct Recovery = 80% Analysis Date = 06/26/12 Pct Recovery = 80% Analysis Date = 06/15/12 Pct Recovery = 80% Analysis Date = 06/15/12 Pct Recovery = 80% Analysis Date = 06/04/12 Pct Recovery = 80% Analysis Date = 06/04/12 Pct Recovery = 80% Analysis Date = 05/24/12 Pct Recovery = 80% Analysis Date = 05/24/12 Pct Recovery = 80% Analysis Date = 05/14/12 Pct Recovery = 80% Analysis Date = 05/14/12 Pct Recovery = 80% Analysis Date = 05/03/12 Pct Recovery = 81% Analysis Date = 05/03/12 Pct Recovery = 81% Analysis Date = 04/22/12 Pct Recovery = 81% Analysis Date = 04/22/12 Pct Recovery = 81% Analysis Date = 04/11/12 Pct Recovery = 81% Analysis Date = 04/11/12 Pct Recovery = 81% Analysis Date = 03/31/12 Pct Recovery = 81% Analysis Date = 03/31/12 Pct Recovery = 81% Analysis Date = 03/21/12 Pct Recovery = 81% Analysis Date = 03/21/12 Pct Recovery = 81% Analysis Date = 03/10/12 Pct Recovery = 82% Analysis Date = 03/10/12 Pct Recovery = 82% Analysis Date = 02/28/12 Pct Recovery = 82% Analysis Date = 02/28/12 Pct Recovery = 82% Analysis Date = 02/17/12 Pct Recovery = 82% Analysis Date = 02/17/12 Pct Recovery = 82% Analysis Date = 02/07/12 Pct Recovery = 82% Analysis Date = 02/07/12 Pct Recovery = 82% Analysis Date = 01/27/12 Pct Recovery = 82% Analysis Date = 01/27/12 Pct Recovery = 82% Analysis Date = 01/16/12 Pct Recovery = 82% Analysis Date = 01/16/12 Pct Recovery = 82% Analysis Date = 01/05/12 Pct Recovery = 83% Analysis Date = 01/05/12 Pct Recovery = 83% Analysis Date = 12/25/11 Pct Recovery = 83% Analysis Date = 12/25/11 Pct Recovery = 83% Analysis Date = 12/15/11 Pct Recovery = 83% Analysis Date = 12/15/11 Pct Recovery = 83% Analysis Date = 12/04/11 Pct Recovery = 83% Analysis Date = 12/04/11 Pct Recovery = 83% Analysis Date = 11/23/11 Pct Recovery = 83% Analysis Date = 11/23/11 Pct Recovery = 83% Analysis Date = 11/12/11 Pct Recovery = 83% Analysis Date = 11/12/11 Pct Recovery = 83% Analysis Date = 11/02/11 Pct Recovery = 83% Analysis Date = 11/02/11 Pct Recovery = 83% Analysis Date = 10/22/11 Pct Recovery = 84% Analysis Date = 10/22/11 Pct Recovery = 84% Analysis Date = 10/11/11 Pct Recovery = 84% Analysis Date = 10/11/11 Pct Recovery = 84% Analysis Date = 09/30/11 Pct Recovery = 84% Analysis Date = 09/30/11 Pct Recovery = 84% Analysis Date = 09/19/11 Pct Recovery = 84% Analysis Date = 09/19/11 Pct Recovery = 84% Analysis Date = 09/09/11 Pct Recovery = 84% Analysis Date = 09/09/11 Pct Recovery = 84% Analysis Date = 08/29/11 Pct Recovery = 84% Analysis Date = 08/29/11 Pct Recovery = 84% Analysis Date = 08/18/11 Pct Recovery = 85% Analysis Date = 08/18/11 Pct Recovery = 85% Analysis Date = 08/07/11 Pct Recovery = 85% Analysis Date = 08/07/11 Pct Recovery = 85% Analysis Date = 07/28/11 Pct Recovery = 85% Analysis Date = 07/28/11 Pct Recovery = 85% Analysis Date = 07/17/11 Pct Recovery = 85% Analysis Date = 07/17/11 Pct Recovery = 85% Analysis Date = 07/06/11 Pct Recovery = 85% Analysis Date = 07/06/11 Pct Recovery = 85% Analysis Date = 06/25/11 Pct Recovery = 85% Analysis Date = 06/25/11 Pct Recovery = 85% Analysis Date = 06/14/11 Pct Recovery = 85% Analysis Date = 06/14/11 Pct Recovery = 85% Analysis Date = 06/04/11 Pct Recovery = 85% Analysis Date = 06/04/11 Pct Recovery = 85% Analysis Date = 05/24/11 Pct Recovery = 86% Analysis Date = 05/24/11 Pct Recovery = 86% Analysis Date = 05/13/11 Pct Recovery = 86% Analysis Date = 05/13/11 Pct Recovery = 86% Analysis Date = 05/02/11 Pct Recovery = 86% Analysis Date = 05/02/11 Pct Recovery = 86% Analysis Date = 04/22/11 Pct Recovery = 86% Analysis Date = 04/22/11 Pct Recovery = 86% Analysis Date = 04/11/11 Pct Recovery = 86% Analysis Date = 04/11/11 Pct Recovery = 86% Analysis Date = 03/31/11 Pct Recovery = 86% Analysis Date = 03/31/11 Pct Recovery = 86% Analysis Date = 03/20/11 Pct Recovery = 86% Analysis Date = 03/20/11 Pct Recovery = 86% Analysis Date = 03/10/11 Pct Recovery = 86% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
CIS-ANDROSTERONE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 1 72% . 72% 0%
>= Reporting Level 50 76% 17% 77% 18%
Total 51 76% 17% 76% 18%

Sample Statistics
CIS-ANDROSTERONE

Characteristic N % % Basis
Plotted 51 78% Spiked
Estimated Values 0 0% Spiked
Deleted Values 2 2% Spiked + Not Spiked
Spiked, Censored 5 8% Spiked
Spiked 65 .  
False Negatives 9 14% 9 out of 65
Not Spiked 66 .  
False Positives 1 2% 1 out of 64

BQS OBSP Determination:
DIHYDROTESTOSTERONE
METHOD: 4434 , TESTIDCODE: 64544GM005
Open Data Set

Analysis Date = 08/31/16 SpikeMix = Spex Organics TS160420010: 50 µl & ChemService 5016200: 50 µl Pct Recovery = 76% Analysis Date = 08/19/16 SpikeMix = Supelco LC20140V: 50 µl & Spex Organics TS160420010: 50 µl Pct Recovery = 148% Analysis Date = 08/11/16 SpikeMix = ChemService 5016100: 50 µl & Spex Organics TS160420010: 50 µl Pct Recovery = 66% Analysis Date = 02/22/13 SpikeMix = Restek A089631: 50 µl & Supelco LB92781: 50 µl Pct Recovery = 64% Analysis Date = 12/18/12 SpikeMix = Spex Organics T1120525010: 50 µl & Supelco LB92781: 50 µl Pct Recovery = 69% Analysis Date = 04/13/15 SpikeMix = Abs 042114: 60 µl & Spex Organics E1140505004: 60 µl Pct Recovery = 75% Analysis Date = 02/12/15 SpikeMix = Supelco LC06946: 60 µl & Abs 042114: 60 µl Pct Recovery = 60% Analysis Date = 08/26/14 SpikeMix = Abs 031014: 60 µl & Abs 042114: 60 µl Pct Recovery = 66% Analysis Date = 08/22/14 SpikeMix = ERA 0227-14-07.2: 60 µl & Abs 042114: 60 µl Pct Recovery = 66% Analysis Date = 03/14/14 SpikeMix = Supelco LB99393: 50 µl & Abs 050813: 50 µl Pct Recovery = 57% Analysis Date = 02/25/14 SpikeMix = ERA 0415-13-01.1A: 50 µl & Abs 050813: 50 µl Pct Recovery = 47% Analysis Date = 03/14/14 SpikeMix = ERA 0415-13-01.2A: 50 µl & Spex Organics T1130423008: 50 µl Pct Recovery = 58% Analysis Date = 03/05/14 SpikeMix = Spex Organics T1130423008: 50 µl & Abs 071513: 50 µl Pct Recovery = 73% Analysis Date = 08/09/13 SpikeMix = ERA 0415-13-01.2A: 50 µl & Spex Organics T1130423008: 50 µl Pct Recovery = 69% Analysis Date = 01/07/16 SpikeMix = Crescent 04EE007: 60 µl & Abs 041515: 60 µl Pct Recovery = 85% Analysis Date = 01/08/16 SpikeMix = Spex Organics EN150501025: 60 µl & ERA 0601-15-04: 60 µl Pct Recovery = 88% Analysis Date = 04/10/13 SpikeMix = ERA 0511-12-02: 25 µl & Supelco LB92781: 25 µl Pct Recovery = 79% Analysis Date = 02/08/13 SpikeMix = ERA 0507-12-04.1: 25 µl & Supelco LB92781: 25 µl Pct Recovery = 73% Analysis Date = 12/18/12 SpikeMix = Restek A089631: 25 µl & Supelco LB92781: 25 µl Pct Recovery = 66% Analysis Date = 03/07/16 SpikeMix = Abs 041515: 50 µl & ERA 0601-15-04: 50 µl Pct Recovery = 87% Analysis Date = 12/10/15 SpikeMix = Abs 041515: 50 µl & ERA 0601-15-04: 50 µl Pct Recovery = 73% Analysis Date = 08/17/15 SpikeMix = ChemService 4073900: 50 µl & Abs 041515: 50 µl Pct Recovery = 55% Analysis Date = 07/12/16 SpikeMix = Spex Organics EN150501025: 50 µl & ERA 0601-15-04: 50 µl Pct Recovery = 86% Analysis Date = 06/24/16 SpikeMix = Crescent 04EE007: 50 µl & Spex Organics EN150501025: 50 µl Pct Recovery = 81% Analysis Date = 01/08/16 SpikeMix = Crescent 04EE007: 50 µl & Spex Organics EN150501025: 50 µl Pct Recovery = 61% Analysis Date = 02/01/17 SpikeMix = Supelco LC20140V: 30 µl & Abs 052616: 30 µl Pct Recovery = 74% Analysis Date = 01/13/17 SpikeMix = Abs 052616: 30 µl & ChemService 5016200: 30 µl Pct Recovery = 74% Analysis Date = 12/29/16 SpikeMix = ChemService 5016100: 30 µl & Abs 052616: 30 µl Pct Recovery = 82% Analysis Date = 12/05/16 SpikeMix = Abs 052616: 30 µl & Abs 061416H: 30 µl Pct Recovery = 90% Analysis Date = 09/15/16 SpikeMix = Supelco LC20140V: 30 µl & Spex Organics EN160621015: 30 µl Pct Recovery = 81% Analysis Date = 12/22/14 SpikeMix = Abs 042114: 30 µl & Abs 031014: 30 µl Pct Recovery = 57% Analysis Date = 12/16/14 SpikeMix = Supelco LC06946: 30 µl & Abs 042114: 30 µl Pct Recovery = 48% Analysis Date = 11/05/14 SpikeMix = ERA 0227-14-07.2: 30 µl & Abs 042114: 30 µl Pct Recovery = 61% Analysis Date = 03/07/16 SpikeMix = ChemService 4073900: 30 µl & Abs 041515: 30 µl Pct Recovery = 97% Analysis Date = 09/23/15 SpikeMix = ChemService 4073900: 30 µl & Spex Organics EN150501025: 30 µl Pct Recovery = 103% Analysis Date = 03/03/14 SpikeMix = Abs 050813: 20 µl & Abs 071513: 20 µl Pct Recovery = 46% Analysis Date = 02/19/14 SpikeMix = Abs 050813: 20 µl & Abs 071513: 20 µl Pct Recovery = 74% Analysis Date = 11/18/13 SpikeMix = ERA 0415-13-01.2A: 20 µl & Abs 050813: 20 µl Pct Recovery = 75% Analysis Date = 12/09/13 SpikeMix = Supelco LB99393: 20 µl & Spex Organics T1130423008: 20 µl Pct Recovery = 51% Analysis Date = 06/27/13 SpikeMix = ERA 0415-13-01.1A: 20 µl & Spex Organics T1130423008: 20 µl Pct Recovery = 54% Analysis Date = 01/31/17 Pct Recovery = 87% Analysis Date = 01/24/17 Pct Recovery = 87% Analysis Date = 01/24/17 Pct Recovery = 87% Analysis Date = 01/16/17 Pct Recovery = 87% Analysis Date = 01/16/17 Pct Recovery = 87% Analysis Date = 01/09/17 Pct Recovery = 87% Analysis Date = 01/09/17 Pct Recovery = 87% Analysis Date = 01/01/17 Pct Recovery = 87% Analysis Date = 01/01/17 Pct Recovery = 87% Analysis Date = 12/25/16 Pct Recovery = 87% Analysis Date = 12/25/16 Pct Recovery = 87% Analysis Date = 12/17/16 Pct Recovery = 86% Analysis Date = 12/17/16 Pct Recovery = 86% Analysis Date = 12/10/16 Pct Recovery = 86% Analysis Date = 12/10/16 Pct Recovery = 86% Analysis Date = 12/02/16 Pct Recovery = 86% Analysis Date = 12/02/16 Pct Recovery = 86% Analysis Date = 11/25/16 Pct Recovery = 86% Analysis Date = 11/25/16 Pct Recovery = 86% Analysis Date = 11/17/16 Pct Recovery = 86% Analysis Date = 11/17/16 Pct Recovery = 86% Analysis Date = 11/10/16 Pct Recovery = 86% Analysis Date = 11/10/16 Pct Recovery = 86% Analysis Date = 11/02/16 Pct Recovery = 86% Analysis Date = 11/02/16 Pct Recovery = 86% Analysis Date = 10/26/16 Pct Recovery = 86% Analysis Date = 10/26/16 Pct Recovery = 86% Analysis Date = 10/18/16 Pct Recovery = 86% Analysis Date = 10/18/16 Pct Recovery = 86% Analysis Date = 10/11/16 Pct Recovery = 86% Analysis Date = 10/11/16 Pct Recovery = 86% Analysis Date = 10/03/16 Pct Recovery = 86% Analysis Date = 10/03/16 Pct Recovery = 86% Analysis Date = 09/25/16 Pct Recovery = 85% Analysis Date = 09/25/16 Pct Recovery = 85% Analysis Date = 09/18/16 Pct Recovery = 85% Analysis Date = 09/18/16 Pct Recovery = 85% Analysis Date = 09/10/16 Pct Recovery = 85% Analysis Date = 09/10/16 Pct Recovery = 85% Analysis Date = 09/03/16 Pct Recovery = 85% Analysis Date = 09/03/16 Pct Recovery = 85% Analysis Date = 08/26/16 Pct Recovery = 85% Analysis Date = 08/26/16 Pct Recovery = 85% Analysis Date = 08/19/16 Pct Recovery = 85% Analysis Date = 08/19/16 Pct Recovery = 85% Analysis Date = 08/11/16 Pct Recovery = 85% Analysis Date = 08/11/16 Pct Recovery = 85% Analysis Date = 08/04/16 Pct Recovery = 85% Analysis Date = 08/04/16 Pct Recovery = 85% Analysis Date = 07/27/16 Pct Recovery = 85% Analysis Date = 07/27/16 Pct Recovery = 85% Analysis Date = 07/20/16 Pct Recovery = 85% Analysis Date = 07/20/16 Pct Recovery = 85% Analysis Date = 07/12/16 Pct Recovery = 84% Analysis Date = 07/12/16 Pct Recovery = 84% Analysis Date = 07/05/16 Pct Recovery = 84% Analysis Date = 07/05/16 Pct Recovery = 84% Analysis Date = 06/27/16 Pct Recovery = 84% Analysis Date = 06/27/16 Pct Recovery = 84% Analysis Date = 06/20/16 Pct Recovery = 84% Analysis Date = 06/20/16 Pct Recovery = 84% Analysis Date = 06/12/16 Pct Recovery = 84% Analysis Date = 06/12/16 Pct Recovery = 84% Analysis Date = 06/05/16 Pct Recovery = 84% Analysis Date = 06/05/16 Pct Recovery = 84% Analysis Date = 05/28/16 Pct Recovery = 84% Analysis Date = 05/28/16 Pct Recovery = 84% Analysis Date = 05/20/16 Pct Recovery = 83% Analysis Date = 05/20/16 Pct Recovery = 83% Analysis Date = 05/13/16 Pct Recovery = 83% Analysis Date = 05/13/16 Pct Recovery = 83% Analysis Date = 05/05/16 Pct Recovery = 83% Analysis Date = 05/05/16 Pct Recovery = 83% Analysis Date = 04/28/16 Pct Recovery = 83% Analysis Date = 04/28/16 Pct Recovery = 83% Analysis Date = 04/20/16 Pct Recovery = 83% Analysis Date = 04/20/16 Pct Recovery = 83% Analysis Date = 04/13/16 Pct Recovery = 83% Analysis Date = 04/13/16 Pct Recovery = 83% Analysis Date = 04/05/16 Pct Recovery = 83% Analysis Date = 04/05/16 Pct Recovery = 83% Analysis Date = 03/29/16 Pct Recovery = 83% Analysis Date = 03/29/16 Pct Recovery = 83% Analysis Date = 03/21/16 Pct Recovery = 82% Analysis Date = 03/21/16 Pct Recovery = 82% Analysis Date = 03/14/16 Pct Recovery = 82% Analysis Date = 03/14/16 Pct Recovery = 82% Analysis Date = 03/06/16 Pct Recovery = 82% Analysis Date = 03/06/16 Pct Recovery = 82% Analysis Date = 02/28/16 Pct Recovery = 82% Analysis Date = 02/28/16 Pct Recovery = 82% Analysis Date = 02/20/16 Pct Recovery = 82% Analysis Date = 02/20/16 Pct Recovery = 82% Analysis Date = 02/13/16 Pct Recovery = 82% Analysis Date = 02/13/16 Pct Recovery = 82% Analysis Date = 02/05/16 Pct Recovery = 81% Analysis Date = 02/05/16 Pct Recovery = 81% Analysis Date = 01/29/16 Pct Recovery = 81% Analysis Date = 01/29/16 Pct Recovery = 81% Analysis Date = 01/21/16 Pct Recovery = 81% Analysis Date = 01/21/16 Pct Recovery = 81% Analysis Date = 01/13/16 Pct Recovery = 81% Analysis Date = 01/13/16 Pct Recovery = 81% Analysis Date = 01/06/16 Pct Recovery = 81% Analysis Date = 01/06/16 Pct Recovery = 81% Analysis Date = 12/29/15 Pct Recovery = 80% Analysis Date = 12/29/15 Pct Recovery = 80% Analysis Date = 12/22/15 Pct Recovery = 80% Analysis Date = 12/22/15 Pct Recovery = 80% Analysis Date = 12/14/15 Pct Recovery = 80% Analysis Date = 12/14/15 Pct Recovery = 80% Analysis Date = 12/07/15 Pct Recovery = 79% Analysis Date = 12/07/15 Pct Recovery = 79% Analysis Date = 11/29/15 Pct Recovery = 79% Analysis Date = 11/29/15 Pct Recovery = 79% Analysis Date = 11/22/15 Pct Recovery = 79% Analysis Date = 11/22/15 Pct Recovery = 79% Analysis Date = 11/14/15 Pct Recovery = 78% Analysis Date = 11/14/15 Pct Recovery = 78% Analysis Date = 11/07/15 Pct Recovery = 78% Analysis Date = 11/07/15 Pct Recovery = 78% Analysis Date = 10/30/15 Pct Recovery = 78% Analysis Date = 10/30/15 Pct Recovery = 78% Analysis Date = 10/23/15 Pct Recovery = 77% Analysis Date = 10/23/15 Pct Recovery = 77% Analysis Date = 10/15/15 Pct Recovery = 77% Analysis Date = 10/15/15 Pct Recovery = 77% Analysis Date = 10/08/15 Pct Recovery = 76% Analysis Date = 10/08/15 Pct Recovery = 76% Analysis Date = 09/30/15 Pct Recovery = 76% Analysis Date = 09/30/15 Pct Recovery = 76% Analysis Date = 09/23/15 Pct Recovery = 76% Analysis Date = 09/23/15 Pct Recovery = 76% Analysis Date = 09/15/15 Pct Recovery = 75% Analysis Date = 09/15/15 Pct Recovery = 75% Analysis Date = 09/07/15 Pct Recovery = 75% Analysis Date = 09/07/15 Pct Recovery = 75% Analysis Date = 08/31/15 Pct Recovery = 74% Analysis Date = 08/31/15 Pct Recovery = 74% Analysis Date = 08/23/15 Pct Recovery = 74% Analysis Date = 08/23/15 Pct Recovery = 74% Analysis Date = 08/16/15 Pct Recovery = 74% Analysis Date = 08/16/15 Pct Recovery = 74% Analysis Date = 08/08/15 Pct Recovery = 73% Analysis Date = 08/08/15 Pct Recovery = 73% Analysis Date = 08/01/15 Pct Recovery = 73% Analysis Date = 08/01/15 Pct Recovery = 73% Analysis Date = 07/24/15 Pct Recovery = 73% Analysis Date = 07/24/15 Pct Recovery = 73% Analysis Date = 07/17/15 Pct Recovery = 73% Analysis Date = 07/17/15 Pct Recovery = 73% Analysis Date = 07/09/15 Pct Recovery = 72% Analysis Date = 07/09/15 Pct Recovery = 72% Analysis Date = 07/02/15 Pct Recovery = 72% Analysis Date = 07/02/15 Pct Recovery = 72% Analysis Date = 06/24/15 Pct Recovery = 72% Analysis Date = 06/24/15 Pct Recovery = 72% Analysis Date = 06/17/15 Pct Recovery = 71% Analysis Date = 06/17/15 Pct Recovery = 71% Analysis Date = 06/09/15 Pct Recovery = 71% Analysis Date = 06/09/15 Pct Recovery = 71% Analysis Date = 06/02/15 Pct Recovery = 71% Analysis Date = 06/02/15 Pct Recovery = 71% Analysis Date = 05/25/15 Pct Recovery = 71% Analysis Date = 05/25/15 Pct Recovery = 71% Analysis Date = 05/18/15 Pct Recovery = 70% Analysis Date = 05/18/15 Pct Recovery = 70% Analysis Date = 05/10/15 Pct Recovery = 70% Analysis Date = 05/10/15 Pct Recovery = 70% Analysis Date = 05/02/15 Pct Recovery = 70% Analysis Date = 05/02/15 Pct Recovery = 70% Analysis Date = 04/25/15 Pct Recovery = 69% Analysis Date = 04/25/15 Pct Recovery = 69% Analysis Date = 04/17/15 Pct Recovery = 69% Analysis Date = 04/17/15 Pct Recovery = 69% Analysis Date = 04/10/15 Pct Recovery = 69% Analysis Date = 04/10/15 Pct Recovery = 69% Analysis Date = 04/02/15 Pct Recovery = 69% Analysis Date = 04/02/15 Pct Recovery = 69% Analysis Date = 03/26/15 Pct Recovery = 68% Analysis Date = 03/26/15 Pct Recovery = 68% Analysis Date = 03/18/15 Pct Recovery = 68% Analysis Date = 03/18/15 Pct Recovery = 68% Analysis Date = 03/11/15 Pct Recovery = 68% Analysis Date = 03/11/15 Pct Recovery = 68% Analysis Date = 03/03/15 Pct Recovery = 67% Analysis Date = 03/03/15 Pct Recovery = 67% Analysis Date = 02/24/15 Pct Recovery = 67% Analysis Date = 02/24/15 Pct Recovery = 67% Analysis Date = 02/16/15 Pct Recovery = 67% Analysis Date = 02/16/15 Pct Recovery = 67% Analysis Date = 02/09/15 Pct Recovery = 67% Analysis Date = 02/09/15 Pct Recovery = 67% Analysis Date = 02/01/15 Pct Recovery = 66% Analysis Date = 02/01/15 Pct Recovery = 66% Analysis Date = 01/25/15 Pct Recovery = 66% Analysis Date = 01/25/15 Pct Recovery = 66% Analysis Date = 01/17/15 Pct Recovery = 66% Analysis Date = 01/17/15 Pct Recovery = 66% Analysis Date = 01/09/15 Pct Recovery = 65% Analysis Date = 01/09/15 Pct Recovery = 65% Analysis Date = 01/02/15 Pct Recovery = 65% Analysis Date = 01/02/15 Pct Recovery = 65% Analysis Date = 12/25/14 Pct Recovery = 65% Analysis Date = 12/25/14 Pct Recovery = 65% Analysis Date = 12/18/14 Pct Recovery = 65% Analysis Date = 12/18/14 Pct Recovery = 65% Analysis Date = 12/10/14 Pct Recovery = 64% Analysis Date = 12/10/14 Pct Recovery = 64% Analysis Date = 12/03/14 Pct Recovery = 64% Analysis Date = 12/03/14 Pct Recovery = 64% Analysis Date = 11/25/14 Pct Recovery = 64% Analysis Date = 11/25/14 Pct Recovery = 64% Analysis Date = 11/18/14 Pct Recovery = 63% Analysis Date = 11/18/14 Pct Recovery = 63% Analysis Date = 11/10/14 Pct Recovery = 63% Analysis Date = 11/10/14 Pct Recovery = 63% Analysis Date = 11/03/14 Pct Recovery = 63% Analysis Date = 11/03/14 Pct Recovery = 63% Analysis Date = 10/26/14 Pct Recovery = 63% Analysis Date = 10/26/14 Pct Recovery = 63% Analysis Date = 10/19/14 Pct Recovery = 63% Analysis Date = 10/19/14 Pct Recovery = 63% Analysis Date = 10/11/14 Pct Recovery = 63% Analysis Date = 10/11/14 Pct Recovery = 63% Analysis Date = 10/04/14 Pct Recovery = 63% Analysis Date = 10/04/14 Pct Recovery = 63% Analysis Date = 09/26/14 Pct Recovery = 63% Analysis Date = 09/26/14 Pct Recovery = 63% Analysis Date = 09/19/14 Pct Recovery = 63% Analysis Date = 09/19/14 Pct Recovery = 63% Analysis Date = 09/11/14 Pct Recovery = 63% Analysis Date = 09/11/14 Pct Recovery = 63% Analysis Date = 09/03/14 Pct Recovery = 63% Analysis Date = 09/03/14 Pct Recovery = 63% Analysis Date = 08/27/14 Pct Recovery = 63% Analysis Date = 08/27/14 Pct Recovery = 63% Analysis Date = 08/19/14 Pct Recovery = 63% Analysis Date = 08/19/14 Pct Recovery = 63% Analysis Date = 08/12/14 Pct Recovery = 62% Analysis Date = 08/12/14 Pct Recovery = 62% Analysis Date = 08/04/14 Pct Recovery = 62% Analysis Date = 08/04/14 Pct Recovery = 62% Analysis Date = 07/28/14 Pct Recovery = 62% Analysis Date = 07/28/14 Pct Recovery = 62% Analysis Date = 07/20/14 Pct Recovery = 62% Analysis Date = 07/20/14 Pct Recovery = 62% Analysis Date = 07/13/14 Pct Recovery = 62% Analysis Date = 07/13/14 Pct Recovery = 62% Analysis Date = 07/05/14 Pct Recovery = 62% Analysis Date = 07/05/14 Pct Recovery = 62% Analysis Date = 06/28/14 Pct Recovery = 62% Analysis Date = 06/28/14 Pct Recovery = 62% Analysis Date = 06/20/14 Pct Recovery = 62% Analysis Date = 06/20/14 Pct Recovery = 62% Analysis Date = 06/13/14 Pct Recovery = 62% Analysis Date = 06/13/14 Pct Recovery = 62% Analysis Date = 06/05/14 Pct Recovery = 62% Analysis Date = 06/05/14 Pct Recovery = 62% Analysis Date = 05/29/14 Pct Recovery = 62% Analysis Date = 05/29/14 Pct Recovery = 62% Analysis Date = 05/21/14 Pct Recovery = 62% Analysis Date = 05/21/14 Pct Recovery = 62% Analysis Date = 05/14/14 Pct Recovery = 62% Analysis Date = 05/14/14 Pct Recovery = 62% Analysis Date = 05/06/14 Pct Recovery = 62% Analysis Date = 05/06/14 Pct Recovery = 62% Analysis Date = 04/28/14 Pct Recovery = 62% Analysis Date = 04/28/14 Pct Recovery = 62% Analysis Date = 04/21/14 Pct Recovery = 62% Analysis Date = 04/21/14 Pct Recovery = 62% Analysis Date = 04/13/14 Pct Recovery = 62% Analysis Date = 04/13/14 Pct Recovery = 62% Analysis Date = 04/06/14 Pct Recovery = 62% Analysis Date = 04/06/14 Pct Recovery = 62% Analysis Date = 03/29/14 Pct Recovery = 62% Analysis Date = 03/29/14 Pct Recovery = 62% Analysis Date = 03/22/14 Pct Recovery = 62% Analysis Date = 03/22/14 Pct Recovery = 62% Analysis Date = 03/14/14 Pct Recovery = 62% Analysis Date = 03/14/14 Pct Recovery = 62% Analysis Date = 03/07/14 Pct Recovery = 62% Analysis Date = 03/07/14 Pct Recovery = 62% Analysis Date = 02/27/14 Pct Recovery = 62% Analysis Date = 02/27/14 Pct Recovery = 62% Analysis Date = 02/20/14 Pct Recovery = 62% Analysis Date = 02/20/14 Pct Recovery = 62% Analysis Date = 02/12/14 Pct Recovery = 62% Analysis Date = 02/12/14 Pct Recovery = 62% Analysis Date = 02/05/14 Pct Recovery = 62% Analysis Date = 02/05/14 Pct Recovery = 62% Analysis Date = 01/28/14 Pct Recovery = 62% Analysis Date = 01/28/14 Pct Recovery = 62% Analysis Date = 01/21/14 Pct Recovery = 62% Analysis Date = 01/21/14 Pct Recovery = 62% Analysis Date = 01/13/14 Pct Recovery = 63% Analysis Date = 01/13/14 Pct Recovery = 63% Analysis Date = 01/06/14 Pct Recovery = 63% Analysis Date = 01/06/14 Pct Recovery = 63% Analysis Date = 12/29/13 Pct Recovery = 63% Analysis Date = 12/29/13 Pct Recovery = 63% Analysis Date = 12/21/13 Pct Recovery = 63% Analysis Date = 12/21/13 Pct Recovery = 63% Analysis Date = 12/14/13 Pct Recovery = 63% Analysis Date = 12/14/13 Pct Recovery = 63% Analysis Date = 12/06/13 Pct Recovery = 63% Analysis Date = 12/06/13 Pct Recovery = 63% Analysis Date = 11/29/13 Pct Recovery = 63% Analysis Date = 11/29/13 Pct Recovery = 63% Analysis Date = 11/21/13 Pct Recovery = 63% Analysis Date = 11/21/13 Pct Recovery = 63% Analysis Date = 11/14/13 Pct Recovery = 63% Analysis Date = 11/14/13 Pct Recovery = 63% Analysis Date = 11/06/13 Pct Recovery = 64% Analysis Date = 11/06/13 Pct Recovery = 64% Analysis Date = 10/30/13 Pct Recovery = 64% Analysis Date = 10/30/13 Pct Recovery = 64% Analysis Date = 10/22/13 Pct Recovery = 64% Analysis Date = 10/22/13 Pct Recovery = 64% Analysis Date = 10/15/13 Pct Recovery = 64% Analysis Date = 10/15/13 Pct Recovery = 64% Analysis Date = 10/07/13 Pct Recovery = 64% Analysis Date = 10/07/13 Pct Recovery = 64% Analysis Date = 09/30/13 Pct Recovery = 64% Analysis Date = 09/30/13 Pct Recovery = 64% Analysis Date = 09/22/13 Pct Recovery = 64% Analysis Date = 09/22/13 Pct Recovery = 64% Analysis Date = 09/15/13 Pct Recovery = 64% Analysis Date = 09/15/13 Pct Recovery = 64% Analysis Date = 09/07/13 Pct Recovery = 64% Analysis Date = 09/07/13 Pct Recovery = 64% Analysis Date = 08/31/13 Pct Recovery = 65% Analysis Date = 08/31/13 Pct Recovery = 65% Analysis Date = 08/23/13 Pct Recovery = 65% Analysis Date = 08/23/13 Pct Recovery = 65% Analysis Date = 08/15/13 Pct Recovery = 65% Analysis Date = 08/15/13 Pct Recovery = 65% Analysis Date = 08/08/13 Pct Recovery = 65% Analysis Date = 08/08/13 Pct Recovery = 65% Analysis Date = 07/31/13 Pct Recovery = 65% Analysis Date = 07/31/13 Pct Recovery = 65% Analysis Date = 07/24/13 Pct Recovery = 65% Analysis Date = 07/24/13 Pct Recovery = 65% Analysis Date = 07/16/13 Pct Recovery = 65% Analysis Date = 07/16/13 Pct Recovery = 65% Analysis Date = 07/09/13 Pct Recovery = 65% Analysis Date = 07/09/13 Pct Recovery = 65% Analysis Date = 07/01/13 Pct Recovery = 66% Analysis Date = 07/01/13 Pct Recovery = 66% Analysis Date = 06/24/13 Pct Recovery = 66% Analysis Date = 06/24/13 Pct Recovery = 66% Analysis Date = 06/16/13 Pct Recovery = 66% Analysis Date = 06/16/13 Pct Recovery = 66% Analysis Date = 06/09/13 Pct Recovery = 66% Analysis Date = 06/09/13 Pct Recovery = 66% Analysis Date = 06/01/13 Pct Recovery = 66% Analysis Date = 06/01/13 Pct Recovery = 66% Analysis Date = 05/25/13 Pct Recovery = 66% Analysis Date = 05/25/13 Pct Recovery = 66% Analysis Date = 05/17/13 Pct Recovery = 66% Analysis Date = 05/17/13 Pct Recovery = 66% Analysis Date = 05/10/13 Pct Recovery = 66% Analysis Date = 05/10/13 Pct Recovery = 66% Analysis Date = 05/02/13 Pct Recovery = 66% Analysis Date = 05/02/13 Pct Recovery = 66% Analysis Date = 04/25/13 Pct Recovery = 67% Analysis Date = 04/25/13 Pct Recovery = 67% Analysis Date = 04/17/13 Pct Recovery = 67% Analysis Date = 04/17/13 Pct Recovery = 67% Analysis Date = 04/09/13 Pct Recovery = 67% Analysis Date = 04/09/13 Pct Recovery = 67% Analysis Date = 04/02/13 Pct Recovery = 67% Analysis Date = 04/02/13 Pct Recovery = 67% Analysis Date = 03/25/13 Pct Recovery = 67% Analysis Date = 03/25/13 Pct Recovery = 67% Analysis Date = 03/18/13 Pct Recovery = 67% Analysis Date = 03/18/13 Pct Recovery = 67% Analysis Date = 03/10/13 Pct Recovery = 67% Analysis Date = 03/10/13 Pct Recovery = 67% Analysis Date = 03/03/13 Pct Recovery = 67% Analysis Date = 03/03/13 Pct Recovery = 67% Analysis Date = 02/23/13 Pct Recovery = 68% Analysis Date = 02/23/13 Pct Recovery = 68% Analysis Date = 02/16/13 Pct Recovery = 68% Analysis Date = 02/16/13 Pct Recovery = 68% Analysis Date = 02/08/13 Pct Recovery = 68% Analysis Date = 02/08/13 Pct Recovery = 68% Analysis Date = 02/01/13 Pct Recovery = 68% Analysis Date = 02/01/13 Pct Recovery = 68% Analysis Date = 01/24/13 Pct Recovery = 68% Analysis Date = 01/24/13 Pct Recovery = 68% Analysis Date = 01/17/13 Pct Recovery = 68% Analysis Date = 01/17/13 Pct Recovery = 68% Analysis Date = 01/09/13 Pct Recovery = 68% Analysis Date = 01/09/13 Pct Recovery = 68% Analysis Date = 01/02/13 Pct Recovery = 69% Analysis Date = 01/02/13 Pct Recovery = 69% Analysis Date = 12/25/12 Pct Recovery = 69% Analysis Date = 12/25/12 Pct Recovery = 69% Analysis Date = 12/18/12 Pct Recovery = 69% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
DIHYDROTESTOSTERONE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 40 72% 18% 73% 15%
Total 40 72% 18% 73% 15%

Sample Statistics
DIHYDROTESTOSTERONE

Characteristic N % % Basis
Plotted 40 82% Spiked
Estimated Values 1 2% Spiked
Deleted Values 2 2% Spiked + Not Spiked
Spiked, Censored 1 2% Spiked
Spiked 50 .  
False Negatives 8 16% 8 out of 49
Not Spiked 81 .  
False Positives 1 1% 1 out of 80

BQS OBSP Determination:
EPITESTOSTERONE
METHOD: 4434 , TESTIDCODE: 64537GM005
Open Data Set

Analysis Date = 08/31/16 SpikeMix = Spex Organics TS160420010: 50 µl & ChemService 5016200: 50 µl Pct Recovery = 85% Analysis Date = 08/19/16 SpikeMix = Supelco LC20140V: 50 µl & Spex Organics TS160420010: 50 µl Pct Recovery = 132% Analysis Date = 08/11/16 SpikeMix = ChemService 5016100: 50 µl & Spex Organics TS160420010: 50 µl Pct Recovery = 61% Analysis Date = 12/03/12 SpikeMix = ERA 0511-12-02: 50 µl & Abs 051512: 50 µl Pct Recovery = 67% Analysis Date = 11/07/12 SpikeMix = ERA 0507-12-04.1: 50 µl & ERA 0511-12-02: 50 µl Pct Recovery = 76% Analysis Date = 08/31/12 SpikeMix = ERA 0511-12-02: 25 µl & Abs 051512: 25 µl Pct Recovery = 73% Analysis Date = 05/09/11 SpikeMix = Abs 081810: 100 µl Pct Recovery = 98% Analysis Date = 04/22/13 SpikeMix = ERA 0507-12-04.1: 50 µl & Restek A089631: 50 µl Pct Recovery = 73% Analysis Date = 04/03/13 SpikeMix = Spex Organics T1120525010: 50 µl & Restek A089631: 50 µl Pct Recovery = 75% Analysis Date = 02/22/13 SpikeMix = Restek A089631: 50 µl & Supelco LB92781: 50 µl Pct Recovery = 62% Analysis Date = 12/18/12 SpikeMix = ERA 0507-12-04.1: 50 µl & Restek A089631: 50 µl Pct Recovery = 78% Analysis Date = 07/02/12 SpikeMix = Abs 081810: 100 µl Pct Recovery = 103% Analysis Date = 04/17/12 SpikeMix = Abs 081810: 100 µl Pct Recovery = 103% Analysis Date = 10/03/11 SpikeMix = Abs 081810: 100 µl Pct Recovery = 90% Analysis Date = 04/10/13 SpikeMix = ERA 0511-12-02: 25 µl & Supelco LB92781: 25 µl Pct Recovery = 73% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120525010: 25 µl & ERA 0511-12-02: 25 µl Pct Recovery = 73% Analysis Date = 04/03/13 SpikeMix = Spex Organics T1120525010: 25 µl & Abs 051512: 25 µl Pct Recovery = 63% Analysis Date = 12/18/12 SpikeMix = Restek A089631: 25 µl & Supelco LB92781: 25 µl Pct Recovery = 73% Analysis Date = 11/01/12 SpikeMix = ERA 0507-12-04.1: 25 µl & Abs 051512: 25 µl Pct Recovery = 76% Analysis Date = 08/24/12 SpikeMix = Abs 051512: 25 µl Pct Recovery = 72% Analysis Date = 04/14/14 SpikeMix = ERA 0415-13-01.1A: 50 µl & Abs 071513: 50 µl Pct Recovery = 72% Analysis Date = 03/14/14 SpikeMix = Supelco LB99393: 50 µl & Abs 060413: 50 µl & Abs 071513: 50 µl Pct Recovery = 50% Analysis Date = 03/05/14 SpikeMix = ERA 0415-13-01.1A: 50 µl & Abs 060413: 50 µl & Abs 071513: 50 µl Pct Recovery = 72% Analysis Date = 03/05/14 SpikeMix = Spex Organics T1130423008: 50 µl & Abs 071513: 50 µl Pct Recovery = 65% Analysis Date = 03/14/14 SpikeMix = ERA 0415-13-01.2A: 50 µl & Spex Organics T1130423008: 50 µl Pct Recovery = 50% Analysis Date = 08/09/13 SpikeMix = ERA 0415-13-01.2A: 50 µl & Spex Organics T1130423008: 50 µl Pct Recovery = 51% Analysis Date = 04/13/15 SpikeMix = Abs 042114: 60 µl & Spex Organics E1140505004: 60 µl Pct Recovery = 83% Analysis Date = 02/12/15 SpikeMix = Supelco LC06946: 60 µl & Abs 042114: 60 µl Pct Recovery = 67% Analysis Date = 08/26/14 SpikeMix = Abs 031014: 60 µl & Abs 042114: 60 µl Pct Recovery = 83% Analysis Date = 08/22/14 SpikeMix = ERA 0227-14-07.2: 60 µl & Abs 042114: 60 µl Pct Recovery = 62% Analysis Date = 01/07/16 SpikeMix = Crescent 04EE007: 60 µl & Abs 041515: 60 µl Pct Recovery = 63% Analysis Date = 01/08/16 SpikeMix = Spex Organics EN150501025: 60 µl & ERA 0601-15-04: 60 µl Pct Recovery = 71% Analysis Date = 03/27/12 SpikeMix = Abs 081810: 25 µl Pct Recovery = 91% Analysis Date = 01/27/12 SpikeMix = Abs 081810: 25 µl Pct Recovery = 64% Analysis Date = 10/12/11 SpikeMix = Abs 081810: 25 µl Pct Recovery = 99% Analysis Date = 06/13/11 SpikeMix = Abs 081810: 25 µl Pct Recovery = 84% Analysis Date = 03/30/11 SpikeMix = Abs 081810: 25 µl Pct Recovery = 87% Analysis Date = 09/16/16 SpikeMix = Spex Organics EN160621015: 30 µl & ChemService 5016200: 30 µl Pct Recovery = 88% Analysis Date = 09/15/16 SpikeMix = Supelco LC20140V: 30 µl & Spex Organics EN160621015: 30 µl Pct Recovery = 75% Analysis Date = 02/01/17 SpikeMix = Supelco LC20140V: 30 µl & Abs 052616: 30 µl Pct Recovery = 70% Analysis Date = 01/13/17 SpikeMix = Abs 052616: 30 µl & ChemService 5016200: 30 µl Pct Recovery = 80% Analysis Date = 12/29/16 SpikeMix = ChemService 5016100: 30 µl & Abs 052616: 30 µl Pct Recovery = 120% Analysis Date = 12/05/16 SpikeMix = Abs 052616: 30 µl & Abs 061416H: 30 µl Pct Recovery = 52% Analysis Date = 03/07/16 SpikeMix = Abs 041515: 50 µl & ERA 0601-15-04: 50 µl Pct Recovery = 50% Analysis Date = 12/10/15 SpikeMix = Abs 041515: 50 µl & ERA 0601-15-04: 50 µl Pct Recovery = 87% Analysis Date = 08/17/15 SpikeMix = ChemService 4073900: 50 µl & Abs 041515: 50 µl Pct Recovery = 69% Analysis Date = 07/12/16 SpikeMix = Spex Organics EN150501025: 50 µl & ERA 0601-15-04: 50 µl Pct Recovery = 62% Analysis Date = 06/24/16 SpikeMix = Crescent 04EE007: 50 µl & Spex Organics EN150501025: 50 µl Pct Recovery = 54% Analysis Date = 01/08/16 SpikeMix = Crescent 04EE007: 50 µl & Spex Organics EN150501025: 50 µl Pct Recovery = 77% Analysis Date = 07/21/15 SpikeMix = Supelco LC13547: 50 µl & Spex Organics EN150501025: 50 µl Pct Recovery = 35% Analysis Date = 03/03/14 SpikeMix = Abs 050813: 20 µl & Abs 071513: 20 µl Pct Recovery = 67% Analysis Date = 02/19/14 SpikeMix = Abs 050813: 20 µl & Abs 071513: 20 µl Pct Recovery = 63% Analysis Date = 04/14/14 SpikeMix = ERA 0415-13-01.1A: 20 µl & ERA 0415-13-01.2A: 20 µl & Abs 060413: 20 µl Pct Recovery = 69% Analysis Date = 01/23/14 SpikeMix = Supelco LB99393: 20 µl & ERA 0415-13-01.2A: 20 µl & Abs 060413: 20 µl Pct Recovery = 59% Analysis Date = 11/18/13 SpikeMix = ERA 0415-13-01.2A: 20 µl & Abs 050813: 20 µl Pct Recovery = 68% Analysis Date = 09/16/13 SpikeMix = ERA 0415-13-01.1A: 20 µl & ERA 0415-13-01.2A: 20 µl & Abs 060413: 20 µl Pct Recovery = 87% Analysis Date = 07/19/13 SpikeMix = Supelco LB99393: 20 µl & ERA 0415-13-01.2A: 20 µl Pct Recovery = 59% Analysis Date = 12/22/14 SpikeMix = Abs 042114: 30 µl & Abs 031014: 30 µl Pct Recovery = 62% Analysis Date = 12/16/14 SpikeMix = Supelco LC06946: 30 µl & Abs 042114: 30 µl Pct Recovery = 66% Analysis Date = 11/05/14 SpikeMix = ERA 0227-14-07.2: 30 µl & Abs 042114: 30 µl Pct Recovery = 76% Analysis Date = 03/07/16 SpikeMix = ChemService 4073900: 30 µl & Abs 041515: 30 µl Pct Recovery = 39% Analysis Date = 03/18/16 SpikeMix = Crescent 04EE007: 30 µl & Spex Organics EN150501025: 30 µl Pct Recovery = 64% Analysis Date = 03/18/16 SpikeMix = Spex Organics EN150501025: 30 µl & Supelco LC13547: 30 µl Pct Recovery = 65% Analysis Date = 12/11/15 SpikeMix = Crescent 04EE007: 30 µl & Spex Organics EN150501025: 30 µl Pct Recovery = 61% Analysis Date = 09/23/15 SpikeMix = ChemService 4073900: 30 µl & Spex Organics EN150501025: 30 µl Pct Recovery = 80% Analysis Date = 01/31/17 Pct Recovery = 80% Analysis Date = 01/21/17 Pct Recovery = 80% Analysis Date = 01/21/17 Pct Recovery = 80% Analysis Date = 01/10/17 Pct Recovery = 79% Analysis Date = 01/10/17 Pct Recovery = 79% Analysis Date = 12/30/16 Pct Recovery = 79% Analysis Date = 12/30/16 Pct Recovery = 79% Analysis Date = 12/20/16 Pct Recovery = 79% Analysis Date = 12/20/16 Pct Recovery = 79% Analysis Date = 12/09/16 Pct Recovery = 78% Analysis Date = 12/09/16 Pct Recovery = 78% Analysis Date = 11/28/16 Pct Recovery = 78% Analysis Date = 11/28/16 Pct Recovery = 78% Analysis Date = 11/18/16 Pct Recovery = 78% Analysis Date = 11/18/16 Pct Recovery = 78% Analysis Date = 11/07/16 Pct Recovery = 77% Analysis Date = 11/07/16 Pct Recovery = 77% Analysis Date = 10/27/16 Pct Recovery = 77% Analysis Date = 10/27/16 Pct Recovery = 77% Analysis Date = 10/17/16 Pct Recovery = 77% Analysis Date = 10/17/16 Pct Recovery = 77% Analysis Date = 10/06/16 Pct Recovery = 77% Analysis Date = 10/06/16 Pct Recovery = 77% Analysis Date = 09/25/16 Pct Recovery = 76% Analysis Date = 09/25/16 Pct Recovery = 76% Analysis Date = 09/15/16 Pct Recovery = 76% Analysis Date = 09/15/16 Pct Recovery = 76% Analysis Date = 09/04/16 Pct Recovery = 76% Analysis Date = 09/04/16 Pct Recovery = 76% Analysis Date = 08/24/16 Pct Recovery = 75% Analysis Date = 08/24/16 Pct Recovery = 75% Analysis Date = 08/14/16 Pct Recovery = 75% Analysis Date = 08/14/16 Pct Recovery = 75% Analysis Date = 08/03/16 Pct Recovery = 75% Analysis Date = 08/03/16 Pct Recovery = 75% Analysis Date = 07/23/16 Pct Recovery = 75% Analysis Date = 07/23/16 Pct Recovery = 75% Analysis Date = 07/13/16 Pct Recovery = 74% Analysis Date = 07/13/16 Pct Recovery = 74% Analysis Date = 07/02/16 Pct Recovery = 74% Analysis Date = 07/02/16 Pct Recovery = 74% Analysis Date = 06/21/16 Pct Recovery = 74% Analysis Date = 06/21/16 Pct Recovery = 74% Analysis Date = 06/11/16 Pct Recovery = 74% Analysis Date = 06/11/16 Pct Recovery = 74% Analysis Date = 05/31/16 Pct Recovery = 73% Analysis Date = 05/31/16 Pct Recovery = 73% Analysis Date = 05/20/16 Pct Recovery = 73% Analysis Date = 05/20/16 Pct Recovery = 73% Analysis Date = 05/10/16 Pct Recovery = 73% Analysis Date = 05/10/16 Pct Recovery = 73% Analysis Date = 04/29/16 Pct Recovery = 73% Analysis Date = 04/29/16 Pct Recovery = 73% Analysis Date = 04/18/16 Pct Recovery = 72% Analysis Date = 04/18/16 Pct Recovery = 72% Analysis Date = 04/08/16 Pct Recovery = 72% Analysis Date = 04/08/16 Pct Recovery = 72% Analysis Date = 03/28/16 Pct Recovery = 72% Analysis Date = 03/28/16 Pct Recovery = 72% Analysis Date = 03/17/16 Pct Recovery = 72% Analysis Date = 03/17/16 Pct Recovery = 72% Analysis Date = 03/07/16 Pct Recovery = 71% Analysis Date = 03/07/16 Pct Recovery = 71% Analysis Date = 02/25/16 Pct Recovery = 71% Analysis Date = 02/25/16 Pct Recovery = 71% Analysis Date = 02/14/16 Pct Recovery = 71% Analysis Date = 02/14/16 Pct Recovery = 71% Analysis Date = 02/04/16 Pct Recovery = 71% Analysis Date = 02/04/16 Pct Recovery = 71% Analysis Date = 01/24/16 Pct Recovery = 70% Analysis Date = 01/24/16 Pct Recovery = 70% Analysis Date = 01/13/16 Pct Recovery = 70% Analysis Date = 01/13/16 Pct Recovery = 70% Analysis Date = 01/03/16 Pct Recovery = 70% Analysis Date = 01/03/16 Pct Recovery = 70% Analysis Date = 12/23/15 Pct Recovery = 70% Analysis Date = 12/23/15 Pct Recovery = 70% Analysis Date = 12/12/15 Pct Recovery = 70% Analysis Date = 12/12/15 Pct Recovery = 70% Analysis Date = 12/01/15 Pct Recovery = 69% Analysis Date = 12/01/15 Pct Recovery = 69% Analysis Date = 11/21/15 Pct Recovery = 69% Analysis Date = 11/21/15 Pct Recovery = 69% Analysis Date = 11/10/15 Pct Recovery = 69% Analysis Date = 11/10/15 Pct Recovery = 69% Analysis Date = 10/30/15 Pct Recovery = 69% Analysis Date = 10/30/15 Pct Recovery = 69% Analysis Date = 10/20/15 Pct Recovery = 69% Analysis Date = 10/20/15 Pct Recovery = 69% Analysis Date = 10/09/15 Pct Recovery = 68% Analysis Date = 10/09/15 Pct Recovery = 68% Analysis Date = 09/28/15 Pct Recovery = 68% Analysis Date = 09/28/15 Pct Recovery = 68% Analysis Date = 09/18/15 Pct Recovery = 68% Analysis Date = 09/18/15 Pct Recovery = 68% Analysis Date = 09/07/15 Pct Recovery = 68% Analysis Date = 09/07/15 Pct Recovery = 68% Analysis Date = 08/27/15 Pct Recovery = 68% Analysis Date = 08/27/15 Pct Recovery = 68% Analysis Date = 08/17/15 Pct Recovery = 68% Analysis Date = 08/17/15 Pct Recovery = 68% Analysis Date = 08/06/15 Pct Recovery = 68% Analysis Date = 08/06/15 Pct Recovery = 68% Analysis Date = 07/26/15 Pct Recovery = 68% Analysis Date = 07/26/15 Pct Recovery = 68% Analysis Date = 07/16/15 Pct Recovery = 68% Analysis Date = 07/16/15 Pct Recovery = 68% Analysis Date = 07/05/15 Pct Recovery = 68% Analysis Date = 07/05/15 Pct Recovery = 68% Analysis Date = 06/24/15 Pct Recovery = 67% Analysis Date = 06/24/15 Pct Recovery = 67% Analysis Date = 06/14/15 Pct Recovery = 67% Analysis Date = 06/14/15 Pct Recovery = 67% Analysis Date = 06/03/15 Pct Recovery = 67% Analysis Date = 06/03/15 Pct Recovery = 67% Analysis Date = 05/23/15 Pct Recovery = 67% Analysis Date = 05/23/15 Pct Recovery = 67% Analysis Date = 05/13/15 Pct Recovery = 67% Analysis Date = 05/13/15 Pct Recovery = 67% Analysis Date = 05/02/15 Pct Recovery = 67% Analysis Date = 05/02/15 Pct Recovery = 67% Analysis Date = 04/21/15 Pct Recovery = 67% Analysis Date = 04/21/15 Pct Recovery = 67% Analysis Date = 04/11/15 Pct Recovery = 67% Analysis Date = 04/11/15 Pct Recovery = 67% Analysis Date = 03/31/15 Pct Recovery = 67% Analysis Date = 03/31/15 Pct Recovery = 67% Analysis Date = 03/20/15 Pct Recovery = 67% Analysis Date = 03/20/15 Pct Recovery = 67% Analysis Date = 03/10/15 Pct Recovery = 67% Analysis Date = 03/10/15 Pct Recovery = 67% Analysis Date = 02/27/15 Pct Recovery = 67% Analysis Date = 02/27/15 Pct Recovery = 67% Analysis Date = 02/16/15 Pct Recovery = 67% Analysis Date = 02/16/15 Pct Recovery = 67% Analysis Date = 02/06/15 Pct Recovery = 67% Analysis Date = 02/06/15 Pct Recovery = 67% Analysis Date = 01/26/15 Pct Recovery = 67% Analysis Date = 01/26/15 Pct Recovery = 67% Analysis Date = 01/15/15 Pct Recovery = 67% Analysis Date = 01/15/15 Pct Recovery = 67% Analysis Date = 01/05/15 Pct Recovery = 67% Analysis Date = 01/05/15 Pct Recovery = 67% Analysis Date = 12/25/14 Pct Recovery = 67% Analysis Date = 12/25/14 Pct Recovery = 67% Analysis Date = 12/14/14 Pct Recovery = 67% Analysis Date = 12/14/14 Pct Recovery = 67% Analysis Date = 12/04/14 Pct Recovery = 67% Analysis Date = 12/04/14 Pct Recovery = 67% Analysis Date = 11/23/14 Pct Recovery = 67% Analysis Date = 11/23/14 Pct Recovery = 67% Analysis Date = 11/12/14 Pct Recovery = 67% Analysis Date = 11/12/14 Pct Recovery = 67% Analysis Date = 11/02/14 Pct Recovery = 67% Analysis Date = 11/02/14 Pct Recovery = 67% Analysis Date = 10/22/14 Pct Recovery = 67% Analysis Date = 10/22/14 Pct Recovery = 67% Analysis Date = 10/11/14 Pct Recovery = 67% Analysis Date = 10/11/14 Pct Recovery = 67% Analysis Date = 09/30/14 Pct Recovery = 67% Analysis Date = 09/30/14 Pct Recovery = 67% Analysis Date = 09/20/14 Pct Recovery = 67% Analysis Date = 09/20/14 Pct Recovery = 67% Analysis Date = 09/09/14 Pct Recovery = 67% Analysis Date = 09/09/14 Pct Recovery = 67% Analysis Date = 08/29/14 Pct Recovery = 67% Analysis Date = 08/29/14 Pct Recovery = 67% Analysis Date = 08/19/14 Pct Recovery = 67% Analysis Date = 08/19/14 Pct Recovery = 67% Analysis Date = 08/08/14 Pct Recovery = 67% Analysis Date = 08/08/14 Pct Recovery = 67% Analysis Date = 07/28/14 Pct Recovery = 67% Analysis Date = 07/28/14 Pct Recovery = 67% Analysis Date = 07/18/14 Pct Recovery = 67% Analysis Date = 07/18/14 Pct Recovery = 67% Analysis Date = 07/07/14 Pct Recovery = 67% Analysis Date = 07/07/14 Pct Recovery = 67% Analysis Date = 06/26/14 Pct Recovery = 67% Analysis Date = 06/26/14 Pct Recovery = 67% Analysis Date = 06/16/14 Pct Recovery = 67% Analysis Date = 06/16/14 Pct Recovery = 67% Analysis Date = 06/05/14 Pct Recovery = 67% Analysis Date = 06/05/14 Pct Recovery = 67% Analysis Date = 05/25/14 Pct Recovery = 67% Analysis Date = 05/25/14 Pct Recovery = 67% Analysis Date = 05/15/14 Pct Recovery = 67% Analysis Date = 05/15/14 Pct Recovery = 67% Analysis Date = 05/04/14 Pct Recovery = 67% Analysis Date = 05/04/14 Pct Recovery = 67% Analysis Date = 04/23/14 Pct Recovery = 67% Analysis Date = 04/23/14 Pct Recovery = 67% Analysis Date = 04/13/14 Pct Recovery = 67% Analysis Date = 04/13/14 Pct Recovery = 67% Analysis Date = 04/02/14 Pct Recovery = 67% Analysis Date = 04/02/14 Pct Recovery = 67% Analysis Date = 03/22/14 Pct Recovery = 67% Analysis Date = 03/22/14 Pct Recovery = 67% Analysis Date = 03/12/14 Pct Recovery = 67% Analysis Date = 03/12/14 Pct Recovery = 67% Analysis Date = 03/01/14 Pct Recovery = 67% Analysis Date = 03/01/14 Pct Recovery = 67% Analysis Date = 02/18/14 Pct Recovery = 67% Analysis Date = 02/18/14 Pct Recovery = 67% Analysis Date = 02/08/14 Pct Recovery = 67% Analysis Date = 02/08/14 Pct Recovery = 67% Analysis Date = 01/28/14 Pct Recovery = 67% Analysis Date = 01/28/14 Pct Recovery = 67% Analysis Date = 01/17/14 Pct Recovery = 67% Analysis Date = 01/17/14 Pct Recovery = 67% Analysis Date = 01/07/14 Pct Recovery = 67% Analysis Date = 01/07/14 Pct Recovery = 67% Analysis Date = 12/27/13 Pct Recovery = 68% Analysis Date = 12/27/13 Pct Recovery = 68% Analysis Date = 12/16/13 Pct Recovery = 68% Analysis Date = 12/16/13 Pct Recovery = 68% Analysis Date = 12/06/13 Pct Recovery = 68% Analysis Date = 12/06/13 Pct Recovery = 68% Analysis Date = 11/25/13 Pct Recovery = 68% Analysis Date = 11/25/13 Pct Recovery = 68% Analysis Date = 11/14/13 Pct Recovery = 68% Analysis Date = 11/14/13 Pct Recovery = 68% Analysis Date = 11/04/13 Pct Recovery = 68% Analysis Date = 11/04/13 Pct Recovery = 68% Analysis Date = 10/24/13 Pct Recovery = 68% Analysis Date = 10/24/13 Pct Recovery = 68% Analysis Date = 10/13/13 Pct Recovery = 68% Analysis Date = 10/13/13 Pct Recovery = 68% Analysis Date = 10/03/13 Pct Recovery = 68% Analysis Date = 10/03/13 Pct Recovery = 68% Analysis Date = 09/22/13 Pct Recovery = 69% Analysis Date = 09/22/13 Pct Recovery = 69% Analysis Date = 09/11/13 Pct Recovery = 69% Analysis Date = 09/11/13 Pct Recovery = 69% Analysis Date = 09/01/13 Pct Recovery = 69% Analysis Date = 09/01/13 Pct Recovery = 69% Analysis Date = 08/21/13 Pct Recovery = 69% Analysis Date = 08/21/13 Pct Recovery = 69% Analysis Date = 08/10/13 Pct Recovery = 69% Analysis Date = 08/10/13 Pct Recovery = 69% Analysis Date = 07/30/13 Pct Recovery = 70% Analysis Date = 07/30/13 Pct Recovery = 70% Analysis Date = 07/20/13 Pct Recovery = 70% Analysis Date = 07/20/13 Pct Recovery = 70% Analysis Date = 07/09/13 Pct Recovery = 70% Analysis Date = 07/09/13 Pct Recovery = 70% Analysis Date = 06/28/13 Pct Recovery = 70% Analysis Date = 06/28/13 Pct Recovery = 70% Analysis Date = 06/18/13 Pct Recovery = 70% Analysis Date = 06/18/13 Pct Recovery = 70% Analysis Date = 06/07/13 Pct Recovery = 71% Analysis Date = 06/07/13 Pct Recovery = 71% Analysis Date = 05/27/13 Pct Recovery = 71% Analysis Date = 05/27/13 Pct Recovery = 71% Analysis Date = 05/17/13 Pct Recovery = 71% Analysis Date = 05/17/13 Pct Recovery = 71% Analysis Date = 05/06/13 Pct Recovery = 71% Analysis Date = 05/06/13 Pct Recovery = 71% Analysis Date = 04/25/13 Pct Recovery = 72% Analysis Date = 04/25/13 Pct Recovery = 72% Analysis Date = 04/15/13 Pct Recovery = 72% Analysis Date = 04/15/13 Pct Recovery = 72% Analysis Date = 04/04/13 Pct Recovery = 72% Analysis Date = 04/04/13 Pct Recovery = 72% Analysis Date = 03/24/13 Pct Recovery = 72% Analysis Date = 03/24/13 Pct Recovery = 72% Analysis Date = 03/14/13 Pct Recovery = 73% Analysis Date = 03/14/13 Pct Recovery = 73% Analysis Date = 03/03/13 Pct Recovery = 73% Analysis Date = 03/03/13 Pct Recovery = 73% Analysis Date = 02/20/13 Pct Recovery = 73% Analysis Date = 02/20/13 Pct Recovery = 73% Analysis Date = 02/10/13 Pct Recovery = 74% Analysis Date = 02/10/13 Pct Recovery = 74% Analysis Date = 01/30/13 Pct Recovery = 74% Analysis Date = 01/30/13 Pct Recovery = 74% Analysis Date = 01/19/13 Pct Recovery = 74% Analysis Date = 01/19/13 Pct Recovery = 74% Analysis Date = 01/09/13 Pct Recovery = 75% Analysis Date = 01/09/13 Pct Recovery = 75% Analysis Date = 12/29/12 Pct Recovery = 75% Analysis Date = 12/29/12 Pct Recovery = 75% Analysis Date = 12/18/12 Pct Recovery = 75% Analysis Date = 12/18/12 Pct Recovery = 75% Analysis Date = 12/08/12 Pct Recovery = 76% Analysis Date = 12/08/12 Pct Recovery = 76% Analysis Date = 11/27/12 Pct Recovery = 76% Analysis Date = 11/27/12 Pct Recovery = 76% Analysis Date = 11/16/12 Pct Recovery = 76% Analysis Date = 11/16/12 Pct Recovery = 76% Analysis Date = 11/06/12 Pct Recovery = 77% Analysis Date = 11/06/12 Pct Recovery = 77% Analysis Date = 10/26/12 Pct Recovery = 77% Analysis Date = 10/26/12 Pct Recovery = 77% Analysis Date = 10/15/12 Pct Recovery = 77% Analysis Date = 10/15/12 Pct Recovery = 77% Analysis Date = 10/05/12 Pct Recovery = 78% Analysis Date = 10/05/12 Pct Recovery = 78% Analysis Date = 09/24/12 Pct Recovery = 78% Analysis Date = 09/24/12 Pct Recovery = 78% Analysis Date = 09/13/12 Pct Recovery = 78% Analysis Date = 09/13/12 Pct Recovery = 78% Analysis Date = 09/03/12 Pct Recovery = 79% Analysis Date = 09/03/12 Pct Recovery = 79% Analysis Date = 08/23/12 Pct Recovery = 79% Analysis Date = 08/23/12 Pct Recovery = 79% Analysis Date = 08/12/12 Pct Recovery = 79% Analysis Date = 08/12/12 Pct Recovery = 79% Analysis Date = 08/02/12 Pct Recovery = 79% Analysis Date = 08/02/12 Pct Recovery = 79% Analysis Date = 07/22/12 Pct Recovery = 80% Analysis Date = 07/22/12 Pct Recovery = 80% Analysis Date = 07/11/12 Pct Recovery = 80% Analysis Date = 07/11/12 Pct Recovery = 80% Analysis Date = 07/01/12 Pct Recovery = 80% Analysis Date = 07/01/12 Pct Recovery = 80% Analysis Date = 06/20/12 Pct Recovery = 81% Analysis Date = 06/20/12 Pct Recovery = 81% Analysis Date = 06/09/12 Pct Recovery = 81% Analysis Date = 06/09/12 Pct Recovery = 81% Analysis Date = 05/29/12 Pct Recovery = 81% Analysis Date = 05/29/12 Pct Recovery = 81% Analysis Date = 05/19/12 Pct Recovery = 82% Analysis Date = 05/19/12 Pct Recovery = 82% Analysis Date = 05/08/12 Pct Recovery = 82% Analysis Date = 05/08/12 Pct Recovery = 82% Analysis Date = 04/27/12 Pct Recovery = 82% Analysis Date = 04/27/12 Pct Recovery = 82% Analysis Date = 04/17/12 Pct Recovery = 83% Analysis Date = 04/17/12 Pct Recovery = 83% Analysis Date = 04/06/12 Pct Recovery = 83% Analysis Date = 04/06/12 Pct Recovery = 83% Analysis Date = 03/26/12 Pct Recovery = 83% Analysis Date = 03/26/12 Pct Recovery = 83% Analysis Date = 03/16/12 Pct Recovery = 84% Analysis Date = 03/16/12 Pct Recovery = 84% Analysis Date = 03/05/12 Pct Recovery = 84% Analysis Date = 03/05/12 Pct Recovery = 84% Analysis Date = 02/23/12 Pct Recovery = 84% Analysis Date = 02/23/12 Pct Recovery = 84% Analysis Date = 02/13/12 Pct Recovery = 85% Analysis Date = 02/13/12 Pct Recovery = 85% Analysis Date = 02/02/12 Pct Recovery = 85% Analysis Date = 02/02/12 Pct Recovery = 85% Analysis Date = 01/22/12 Pct Recovery = 85% Analysis Date = 01/22/12 Pct Recovery = 85% Analysis Date = 01/12/12 Pct Recovery = 86% Analysis Date = 01/12/12 Pct Recovery = 86% Analysis Date = 01/01/12 Pct Recovery = 86% Analysis Date = 01/01/12 Pct Recovery = 86% Analysis Date = 12/21/11 Pct Recovery = 86% Analysis Date = 12/21/11 Pct Recovery = 86% Analysis Date = 12/11/11 Pct Recovery = 87% Analysis Date = 12/11/11 Pct Recovery = 87% Analysis Date = 11/30/11 Pct Recovery = 87% Analysis Date = 11/30/11 Pct Recovery = 87% Analysis Date = 11/19/11 Pct Recovery = 87% Analysis Date = 11/19/11 Pct Recovery = 87% Analysis Date = 11/09/11 Pct Recovery = 88% Analysis Date = 11/09/11 Pct Recovery = 88% Analysis Date = 10/29/11 Pct Recovery = 88% Analysis Date = 10/29/11 Pct Recovery = 88% Analysis Date = 10/18/11 Pct Recovery = 88% Analysis Date = 10/18/11 Pct Recovery = 88% Analysis Date = 10/08/11 Pct Recovery = 89% Analysis Date = 10/08/11 Pct Recovery = 89% Analysis Date = 09/27/11 Pct Recovery = 89% Analysis Date = 09/27/11 Pct Recovery = 89% Analysis Date = 09/16/11 Pct Recovery = 89% Analysis Date = 09/16/11 Pct Recovery = 89% Analysis Date = 09/06/11 Pct Recovery = 90% Analysis Date = 09/06/11 Pct Recovery = 90% Analysis Date = 08/26/11 Pct Recovery = 90% Analysis Date = 08/26/11 Pct Recovery = 90% Analysis Date = 08/15/11 Pct Recovery = 90% Analysis Date = 08/15/11 Pct Recovery = 90% Analysis Date = 08/05/11 Pct Recovery = 91% Analysis Date = 08/05/11 Pct Recovery = 91% Analysis Date = 07/25/11 Pct Recovery = 91% Analysis Date = 07/25/11 Pct Recovery = 91% Analysis Date = 07/14/11 Pct Recovery = 91% Analysis Date = 07/14/11 Pct Recovery = 91% Analysis Date = 07/04/11 Pct Recovery = 92% Analysis Date = 07/04/11 Pct Recovery = 92% Analysis Date = 06/23/11 Pct Recovery = 92% Analysis Date = 06/23/11 Pct Recovery = 92% Analysis Date = 06/12/11 Pct Recovery = 92% Analysis Date = 06/12/11 Pct Recovery = 92% Analysis Date = 06/02/11 Pct Recovery = 93% Analysis Date = 06/02/11 Pct Recovery = 93% Analysis Date = 05/22/11 Pct Recovery = 93% Analysis Date = 05/22/11 Pct Recovery = 93% Analysis Date = 05/11/11 Pct Recovery = 93% Analysis Date = 05/11/11 Pct Recovery = 93% Analysis Date = 05/01/11 Pct Recovery = 94% Analysis Date = 05/01/11 Pct Recovery = 94% Analysis Date = 04/20/11 Pct Recovery = 94% Analysis Date = 04/20/11 Pct Recovery = 94% Analysis Date = 04/09/11 Pct Recovery = 94% Analysis Date = 04/09/11 Pct Recovery = 94% Analysis Date = 03/30/11 Pct Recovery = 95% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
EPITESTOSTERONE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 65 73% 17% 72% 13%
Total 65 73% 17% 72% 13%

Sample Statistics
EPITESTOSTERONE

Characteristic N % % Basis
Plotted 65 96% Spiked
Estimated Values 2 3% Spiked
Deleted Values 2 2% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 70 .  
False Negatives 3 4% 3 out of 68
Not Spiked 61 .  
False Positives 0 0% 0 out of 61

BQS OBSP Determination:
EQUILENIN
METHOD: 4434 , TESTIDCODE: 64538GM005
Open Data Set

Analysis Date = 05/09/11 SpikeMix = Abs 081810: 100 µl Pct Recovery = 90% Analysis Date = 07/02/12 SpikeMix = Abs 081810: 100 µl Pct Recovery = 109% Analysis Date = 04/17/12 SpikeMix = Abs 081810: 100 µl Pct Recovery = 102% Analysis Date = 10/03/11 SpikeMix = Abs 081810: 100 µl Pct Recovery = 80% Analysis Date = 04/14/14 SpikeMix = ERA 0415-13-01.1A: 50 µl & Abs 071513: 50 µl Pct Recovery = 53% Analysis Date = 03/14/14 SpikeMix = Supelco LB99393: 50 µl & Abs 060413: 50 µl & Abs 071513: 50 µl Pct Recovery = 40% Analysis Date = 03/05/14 SpikeMix = ERA 0415-13-01.1A: 50 µl & Abs 060413: 50 µl & Abs 071513: 50 µl Pct Recovery = 57% Analysis Date = 11/07/12 SpikeMix = ERA 0507-12-04.1: 50 µl & ERA 0511-12-02: 50 µl Pct Recovery = 56% Analysis Date = 08/19/16 SpikeMix = Supelco LC20140V: 50 µl & Spex Organics TS160420010: 50 µl Pct Recovery = 93% Analysis Date = 12/09/14 SpikeMix = Abs 031014: 60 µl & Supelco LC06946: 60 µl Pct Recovery = 123% Analysis Date = 08/26/14 SpikeMix = Abs 031014: 60 µl & Abs 042114: 60 µl Pct Recovery = 125% Analysis Date = 08/11/14 SpikeMix = Abs 031014: 60 µl & ERA 0227-14-07.2: 60 µl Pct Recovery = 175% Analysis Date = 05/06/14 SpikeMix = Abs 031014: 60 µl & ChemService 2561700: 60 µl Pct Recovery = 152% Analysis Date = 01/08/16 SpikeMix = Spex Organics EN150501025: 60 µl & ERA 0601-15-04: 60 µl Pct Recovery = 59% Analysis Date = 03/07/16 SpikeMix = Abs 041515: 50 µl & ERA 0601-15-04: 50 µl Pct Recovery = 75% Analysis Date = 12/10/15 SpikeMix = Abs 041515: 50 µl & ERA 0601-15-04: 50 µl Pct Recovery = 39% Analysis Date = 08/10/15 SpikeMix = ERA 0601-15-04: 50 µl & Crescent 04EE007: 50 µl Pct Recovery = 158% Analysis Date = 02/01/17 SpikeMix = Supelco LC20140V: 30 µl & Abs 052616: 30 µl Pct Recovery = 110% Analysis Date = 09/15/16 SpikeMix = Supelco LC20140V: 30 µl & Spex Organics EN160621015: 30 µl Pct Recovery = 102% Analysis Date = 09/09/16 SpikeMix = ChemService 5016200: 30 µl & Supelco LC20140V: 30 µl Pct Recovery = 118% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120525010: 25 µl & ERA 0511-12-02: 25 µl Pct Recovery = 73% Analysis Date = 03/27/12 SpikeMix = Abs 081810: 25 µl Pct Recovery = 80% Analysis Date = 01/27/12 SpikeMix = Abs 081810: 25 µl Pct Recovery = 98% Analysis Date = 10/12/11 SpikeMix = Abs 081810: 25 µl Pct Recovery = 89% Analysis Date = 06/13/11 SpikeMix = Abs 081810: 25 µl Pct Recovery = 68% Analysis Date = 03/30/11 SpikeMix = Abs 081810: 25 µl Pct Recovery = 73% Analysis Date = 06/03/15 SpikeMix = Abs 031014: 30 µl & ERA 0227-14-07.2: 30 µl Pct Recovery = 81% Analysis Date = 01/29/15 SpikeMix = Abs 031014: 30 µl & Supelco LC06946: 30 µl Pct Recovery = 117% Analysis Date = 12/22/14 SpikeMix = Abs 042114: 30 µl & Abs 031014: 30 µl Pct Recovery = 125% Analysis Date = 07/14/14 SpikeMix = ERA 0227-14-07.2: 30 µl & Abs 031014: 30 µl Pct Recovery = 116% Analysis Date = 05/14/14 SpikeMix = Abs 031014: 30 µl & ChemService 2561700: 30 µl Pct Recovery = 115% Analysis Date = 04/14/14 SpikeMix = ERA 0415-13-01.1A: 20 µl & ERA 0415-13-01.2A: 20 µl & Abs 060413: 20 µl Pct Recovery = 29% Analysis Date = 01/23/14 SpikeMix = Supelco LB99393: 20 µl & ERA 0415-13-01.2A: 20 µl & Abs 060413: 20 µl Pct Recovery = 51% Analysis Date = 09/16/13 SpikeMix = ERA 0415-13-01.1A: 20 µl & ERA 0415-13-01.2A: 20 µl & Abs 060413: 20 µl Pct Recovery = 61% Analysis Date = 07/19/13 SpikeMix = Supelco LB99393: 20 µl & ERA 0415-13-01.2A: 20 µl Pct Recovery = 42% Analysis Date = 01/08/16 SpikeMix = ERA 0601-15-04: 30 µl & Crescent 04EE007: 30 µl Pct Recovery = 130% Analysis Date = 01/31/17 Pct Recovery = 96% Analysis Date = 01/21/17 Pct Recovery = 96% Analysis Date = 01/21/17 Pct Recovery = 96% Analysis Date = 01/10/17 Pct Recovery = 96% Analysis Date = 01/10/17 Pct Recovery = 96% Analysis Date = 12/30/16 Pct Recovery = 96% Analysis Date = 12/30/16 Pct Recovery = 96% Analysis Date = 12/20/16 Pct Recovery = 96% Analysis Date = 12/20/16 Pct Recovery = 96% Analysis Date = 12/09/16 Pct Recovery = 96% Analysis Date = 12/09/16 Pct Recovery = 96% Analysis Date = 11/28/16 Pct Recovery = 97% Analysis Date = 11/28/16 Pct Recovery = 97% Analysis Date = 11/18/16 Pct Recovery = 97% Analysis Date = 11/18/16 Pct Recovery = 97% Analysis Date = 11/07/16 Pct Recovery = 97% Analysis Date = 11/07/16 Pct Recovery = 97% Analysis Date = 10/27/16 Pct Recovery = 97% Analysis Date = 10/27/16 Pct Recovery = 97% Analysis Date = 10/17/16 Pct Recovery = 97% Analysis Date = 10/17/16 Pct Recovery = 97% Analysis Date = 10/06/16 Pct Recovery = 97% Analysis Date = 10/06/16 Pct Recovery = 97% Analysis Date = 09/25/16 Pct Recovery = 97% Analysis Date = 09/25/16 Pct Recovery = 97% Analysis Date = 09/15/16 Pct Recovery = 97% Analysis Date = 09/15/16 Pct Recovery = 97% Analysis Date = 09/04/16 Pct Recovery = 97% Analysis Date = 09/04/16 Pct Recovery = 97% Analysis Date = 08/24/16 Pct Recovery = 97% Analysis Date = 08/24/16 Pct Recovery = 97% Analysis Date = 08/14/16 Pct Recovery = 98% Analysis Date = 08/14/16 Pct Recovery = 98% Analysis Date = 08/03/16 Pct Recovery = 98% Analysis Date = 08/03/16 Pct Recovery = 98% Analysis Date = 07/23/16 Pct Recovery = 98% Analysis Date = 07/23/16 Pct Recovery = 98% Analysis Date = 07/13/16 Pct Recovery = 98% Analysis Date = 07/13/16 Pct Recovery = 98% Analysis Date = 07/02/16 Pct Recovery = 98% Analysis Date = 07/02/16 Pct Recovery = 98% Analysis Date = 06/21/16 Pct Recovery = 98% Analysis Date = 06/21/16 Pct Recovery = 98% Analysis Date = 06/11/16 Pct Recovery = 98% Analysis Date = 06/11/16 Pct Recovery = 98% Analysis Date = 05/31/16 Pct Recovery = 98% Analysis Date = 05/31/16 Pct Recovery = 98% Analysis Date = 05/20/16 Pct Recovery = 98% Analysis Date = 05/20/16 Pct Recovery = 98% Analysis Date = 05/10/16 Pct Recovery = 98% Analysis Date = 05/10/16 Pct Recovery = 98% Analysis Date = 04/29/16 Pct Recovery = 99% Analysis Date = 04/29/16 Pct Recovery = 99% Analysis Date = 04/18/16 Pct Recovery = 99% Analysis Date = 04/18/16 Pct Recovery = 99% Analysis Date = 04/08/16 Pct Recovery = 99% Analysis Date = 04/08/16 Pct Recovery = 99% Analysis Date = 03/28/16 Pct Recovery = 99% Analysis Date = 03/28/16 Pct Recovery = 99% Analysis Date = 03/17/16 Pct Recovery = 99% Analysis Date = 03/17/16 Pct Recovery = 99% Analysis Date = 03/07/16 Pct Recovery = 99% Analysis Date = 03/07/16 Pct Recovery = 99% Analysis Date = 02/25/16 Pct Recovery = 99% Analysis Date = 02/25/16 Pct Recovery = 99% Analysis Date = 02/14/16 Pct Recovery = 99% Analysis Date = 02/14/16 Pct Recovery = 99% Analysis Date = 02/04/16 Pct Recovery = 100% Analysis Date = 02/04/16 Pct Recovery = 100% Analysis Date = 01/24/16 Pct Recovery = 100% Analysis Date = 01/24/16 Pct Recovery = 100% Analysis Date = 01/13/16 Pct Recovery = 100% Analysis Date = 01/13/16 Pct Recovery = 100% Analysis Date = 01/03/16 Pct Recovery = 100% Analysis Date = 01/03/16 Pct Recovery = 100% Analysis Date = 12/23/15 Pct Recovery = 101% Analysis Date = 12/23/15 Pct Recovery = 101% Analysis Date = 12/12/15 Pct Recovery = 101% Analysis Date = 12/12/15 Pct Recovery = 101% Analysis Date = 12/01/15 Pct Recovery = 101% Analysis Date = 12/01/15 Pct Recovery = 101% Analysis Date = 11/21/15 Pct Recovery = 102% Analysis Date = 11/21/15 Pct Recovery = 102% Analysis Date = 11/10/15 Pct Recovery = 102% Analysis Date = 11/10/15 Pct Recovery = 102% Analysis Date = 10/30/15 Pct Recovery = 102% Analysis Date = 10/30/15 Pct Recovery = 102% Analysis Date = 10/20/15 Pct Recovery = 103% Analysis Date = 10/20/15 Pct Recovery = 103% Analysis Date = 10/09/15 Pct Recovery = 103% Analysis Date = 10/09/15 Pct Recovery = 103% Analysis Date = 09/28/15 Pct Recovery = 103% Analysis Date = 09/28/15 Pct Recovery = 103% Analysis Date = 09/18/15 Pct Recovery = 104% Analysis Date = 09/18/15 Pct Recovery = 104% Analysis Date = 09/07/15 Pct Recovery = 104% Analysis Date = 09/07/15 Pct Recovery = 104% Analysis Date = 08/27/15 Pct Recovery = 104% Analysis Date = 08/27/15 Pct Recovery = 104% Analysis Date = 08/17/15 Pct Recovery = 104% Analysis Date = 08/17/15 Pct Recovery = 104% Analysis Date = 08/06/15 Pct Recovery = 105% Analysis Date = 08/06/15 Pct Recovery = 105% Analysis Date = 07/26/15 Pct Recovery = 105% Analysis Date = 07/26/15 Pct Recovery = 105% Analysis Date = 07/16/15 Pct Recovery = 105% Analysis Date = 07/16/15 Pct Recovery = 105% Analysis Date = 07/05/15 Pct Recovery = 106% Analysis Date = 07/05/15 Pct Recovery = 106% Analysis Date = 06/24/15 Pct Recovery = 106% Analysis Date = 06/24/15 Pct Recovery = 106% Analysis Date = 06/14/15 Pct Recovery = 106% Analysis Date = 06/14/15 Pct Recovery = 106% Analysis Date = 06/03/15 Pct Recovery = 107% Analysis Date = 06/03/15 Pct Recovery = 107% Analysis Date = 05/23/15 Pct Recovery = 107% Analysis Date = 05/23/15 Pct Recovery = 107% Analysis Date = 05/13/15 Pct Recovery = 107% Analysis Date = 05/13/15 Pct Recovery = 107% Analysis Date = 05/02/15 Pct Recovery = 106% Analysis Date = 05/02/15 Pct Recovery = 106% Analysis Date = 04/21/15 Pct Recovery = 106% Analysis Date = 04/21/15 Pct Recovery = 106% Analysis Date = 04/11/15 Pct Recovery = 106% Analysis Date = 04/11/15 Pct Recovery = 106% Analysis Date = 03/31/15 Pct Recovery = 106% Analysis Date = 03/31/15 Pct Recovery = 106% Analysis Date = 03/20/15 Pct Recovery = 106% Analysis Date = 03/20/15 Pct Recovery = 106% Analysis Date = 03/10/15 Pct Recovery = 106% Analysis Date = 03/10/15 Pct Recovery = 106% Analysis Date = 02/27/15 Pct Recovery = 106% Analysis Date = 02/27/15 Pct Recovery = 106% Analysis Date = 02/16/15 Pct Recovery = 105% Analysis Date = 02/16/15 Pct Recovery = 105% Analysis Date = 02/06/15 Pct Recovery = 105% Analysis Date = 02/06/15 Pct Recovery = 105% Analysis Date = 01/26/15 Pct Recovery = 105% Analysis Date = 01/26/15 Pct Recovery = 105% Analysis Date = 01/15/15 Pct Recovery = 105% Analysis Date = 01/15/15 Pct Recovery = 105% Analysis Date = 01/05/15 Pct Recovery = 105% Analysis Date = 01/05/15 Pct Recovery = 105% Analysis Date = 12/25/14 Pct Recovery = 105% Analysis Date = 12/25/14 Pct Recovery = 105% Analysis Date = 12/14/14 Pct Recovery = 105% Analysis Date = 12/14/14 Pct Recovery = 105% Analysis Date = 12/04/14 Pct Recovery = 104% Analysis Date = 12/04/14 Pct Recovery = 104% Analysis Date = 11/23/14 Pct Recovery = 104% Analysis Date = 11/23/14 Pct Recovery = 104% Analysis Date = 11/12/14 Pct Recovery = 104% Analysis Date = 11/12/14 Pct Recovery = 104% Analysis Date = 11/02/14 Pct Recovery = 104% Analysis Date = 11/02/14 Pct Recovery = 104% Analysis Date = 10/22/14 Pct Recovery = 104% Analysis Date = 10/22/14 Pct Recovery = 104% Analysis Date = 10/11/14 Pct Recovery = 104% Analysis Date = 10/11/14 Pct Recovery = 104% Analysis Date = 09/30/14 Pct Recovery = 104% Analysis Date = 09/30/14 Pct Recovery = 104% Analysis Date = 09/20/14 Pct Recovery = 104% Analysis Date = 09/20/14 Pct Recovery = 104% Analysis Date = 09/09/14 Pct Recovery = 103% Analysis Date = 09/09/14 Pct Recovery = 103% Analysis Date = 08/29/14 Pct Recovery = 103% Analysis Date = 08/29/14 Pct Recovery = 103% Analysis Date = 08/19/14 Pct Recovery = 102% Analysis Date = 08/19/14 Pct Recovery = 102% Analysis Date = 08/08/14 Pct Recovery = 101% Analysis Date = 08/08/14 Pct Recovery = 101% Analysis Date = 07/28/14 Pct Recovery = 100% Analysis Date = 07/28/14 Pct Recovery = 100% Analysis Date = 07/18/14 Pct Recovery = 99% Analysis Date = 07/18/14 Pct Recovery = 99% Analysis Date = 07/07/14 Pct Recovery = 98% Analysis Date = 07/07/14 Pct Recovery = 98% Analysis Date = 06/26/14 Pct Recovery = 96% Analysis Date = 06/26/14 Pct Recovery = 96% Analysis Date = 06/16/14 Pct Recovery = 95% Analysis Date = 06/16/14 Pct Recovery = 95% Analysis Date = 06/05/14 Pct Recovery = 94% Analysis Date = 06/05/14 Pct Recovery = 94% Analysis Date = 05/25/14 Pct Recovery = 92% Analysis Date = 05/25/14 Pct Recovery = 92% Analysis Date = 05/15/14 Pct Recovery = 91% Analysis Date = 05/15/14 Pct Recovery = 91% Analysis Date = 05/04/14 Pct Recovery = 89% Analysis Date = 05/04/14 Pct Recovery = 89% Analysis Date = 04/23/14 Pct Recovery = 88% Analysis Date = 04/23/14 Pct Recovery = 88% Analysis Date = 04/13/14 Pct Recovery = 87% Analysis Date = 04/13/14 Pct Recovery = 87% Analysis Date = 04/02/14 Pct Recovery = 86% Analysis Date = 04/02/14 Pct Recovery = 86% Analysis Date = 03/22/14 Pct Recovery = 85% Analysis Date = 03/22/14 Pct Recovery = 85% Analysis Date = 03/12/14 Pct Recovery = 83% Analysis Date = 03/12/14 Pct Recovery = 83% Analysis Date = 03/01/14 Pct Recovery = 82% Analysis Date = 03/01/14 Pct Recovery = 82% Analysis Date = 02/18/14 Pct Recovery = 81% Analysis Date = 02/18/14 Pct Recovery = 81% Analysis Date = 02/08/14 Pct Recovery = 80% Analysis Date = 02/08/14 Pct Recovery = 80% Analysis Date = 01/28/14 Pct Recovery = 79% Analysis Date = 01/28/14 Pct Recovery = 79% Analysis Date = 01/17/14 Pct Recovery = 78% Analysis Date = 01/17/14 Pct Recovery = 78% Analysis Date = 01/07/14 Pct Recovery = 78% Analysis Date = 01/07/14 Pct Recovery = 78% Analysis Date = 12/27/13 Pct Recovery = 77% Analysis Date = 12/27/13 Pct Recovery = 77% Analysis Date = 12/16/13 Pct Recovery = 76% Analysis Date = 12/16/13 Pct Recovery = 76% Analysis Date = 12/06/13 Pct Recovery = 76% Analysis Date = 12/06/13 Pct Recovery = 76% Analysis Date = 11/25/13 Pct Recovery = 75% Analysis Date = 11/25/13 Pct Recovery = 75% Analysis Date = 11/14/13 Pct Recovery = 75% Analysis Date = 11/14/13 Pct Recovery = 75% Analysis Date = 11/04/13 Pct Recovery = 74% Analysis Date = 11/04/13 Pct Recovery = 74% Analysis Date = 10/24/13 Pct Recovery = 73% Analysis Date = 10/24/13 Pct Recovery = 73% Analysis Date = 10/13/13 Pct Recovery = 73% Analysis Date = 10/13/13 Pct Recovery = 73% Analysis Date = 10/03/13 Pct Recovery = 72% Analysis Date = 10/03/13 Pct Recovery = 72% Analysis Date = 09/22/13 Pct Recovery = 71% Analysis Date = 09/22/13 Pct Recovery = 71% Analysis Date = 09/11/13 Pct Recovery = 71% Analysis Date = 09/11/13 Pct Recovery = 71% Analysis Date = 09/01/13 Pct Recovery = 70% Analysis Date = 09/01/13 Pct Recovery = 70% Analysis Date = 08/21/13 Pct Recovery = 70% Analysis Date = 08/21/13 Pct Recovery = 70% Analysis Date = 08/10/13 Pct Recovery = 69% Analysis Date = 08/10/13 Pct Recovery = 69% Analysis Date = 07/30/13 Pct Recovery = 68% Analysis Date = 07/30/13 Pct Recovery = 68% Analysis Date = 07/20/13 Pct Recovery = 68% Analysis Date = 07/20/13 Pct Recovery = 68% Analysis Date = 07/09/13 Pct Recovery = 68% Analysis Date = 07/09/13 Pct Recovery = 68% Analysis Date = 06/28/13 Pct Recovery = 68% Analysis Date = 06/28/13 Pct Recovery = 68% Analysis Date = 06/18/13 Pct Recovery = 68% Analysis Date = 06/18/13 Pct Recovery = 68% Analysis Date = 06/07/13 Pct Recovery = 69% Analysis Date = 06/07/13 Pct Recovery = 69% Analysis Date = 05/27/13 Pct Recovery = 69% Analysis Date = 05/27/13 Pct Recovery = 69% Analysis Date = 05/17/13 Pct Recovery = 69% Analysis Date = 05/17/13 Pct Recovery = 69% Analysis Date = 05/06/13 Pct Recovery = 70% Analysis Date = 05/06/13 Pct Recovery = 70% Analysis Date = 04/25/13 Pct Recovery = 70% Analysis Date = 04/25/13 Pct Recovery = 70% Analysis Date = 04/15/13 Pct Recovery = 70% Analysis Date = 04/15/13 Pct Recovery = 70% Analysis Date = 04/04/13 Pct Recovery = 71% Analysis Date = 04/04/13 Pct Recovery = 71% Analysis Date = 03/24/13 Pct Recovery = 71% Analysis Date = 03/24/13 Pct Recovery = 71% Analysis Date = 03/14/13 Pct Recovery = 71% Analysis Date = 03/14/13 Pct Recovery = 71% Analysis Date = 03/03/13 Pct Recovery = 71% Analysis Date = 03/03/13 Pct Recovery = 71% Analysis Date = 02/20/13 Pct Recovery = 72% Analysis Date = 02/20/13 Pct Recovery = 72% Analysis Date = 02/10/13 Pct Recovery = 72% Analysis Date = 02/10/13 Pct Recovery = 72% Analysis Date = 01/30/13 Pct Recovery = 72% Analysis Date = 01/30/13 Pct Recovery = 72% Analysis Date = 01/19/13 Pct Recovery = 73% Analysis Date = 01/19/13 Pct Recovery = 73% Analysis Date = 01/09/13 Pct Recovery = 73% Analysis Date = 01/09/13 Pct Recovery = 73% Analysis Date = 12/29/12 Pct Recovery = 73% Analysis Date = 12/29/12 Pct Recovery = 73% Analysis Date = 12/18/12 Pct Recovery = 74% Analysis Date = 12/18/12 Pct Recovery = 74% Analysis Date = 12/08/12 Pct Recovery = 74% Analysis Date = 12/08/12 Pct Recovery = 74% Analysis Date = 11/27/12 Pct Recovery = 74% Analysis Date = 11/27/12 Pct Recovery = 74% Analysis Date = 11/16/12 Pct Recovery = 74% Analysis Date = 11/16/12 Pct Recovery = 74% Analysis Date = 11/06/12 Pct Recovery = 75% Analysis Date = 11/06/12 Pct Recovery = 75% Analysis Date = 10/26/12 Pct Recovery = 75% Analysis Date = 10/26/12 Pct Recovery = 75% Analysis Date = 10/15/12 Pct Recovery = 75% Analysis Date = 10/15/12 Pct Recovery = 75% Analysis Date = 10/05/12 Pct Recovery = 76% Analysis Date = 10/05/12 Pct Recovery = 76% Analysis Date = 09/24/12 Pct Recovery = 76% Analysis Date = 09/24/12 Pct Recovery = 76% Analysis Date = 09/13/12 Pct Recovery = 76% Analysis Date = 09/13/12 Pct Recovery = 76% Analysis Date = 09/03/12 Pct Recovery = 77% Analysis Date = 09/03/12 Pct Recovery = 77% Analysis Date = 08/23/12 Pct Recovery = 77% Analysis Date = 08/23/12 Pct Recovery = 77% Analysis Date = 08/12/12 Pct Recovery = 77% Analysis Date = 08/12/12 Pct Recovery = 77% Analysis Date = 08/02/12 Pct Recovery = 77% Analysis Date = 08/02/12 Pct Recovery = 77% Analysis Date = 07/22/12 Pct Recovery = 78% Analysis Date = 07/22/12 Pct Recovery = 78% Analysis Date = 07/11/12 Pct Recovery = 78% Analysis Date = 07/11/12 Pct Recovery = 78% Analysis Date = 07/01/12 Pct Recovery = 78% Analysis Date = 07/01/12 Pct Recovery = 78% Analysis Date = 06/20/12 Pct Recovery = 79% Analysis Date = 06/20/12 Pct Recovery = 79% Analysis Date = 06/09/12 Pct Recovery = 79% Analysis Date = 06/09/12 Pct Recovery = 79% Analysis Date = 05/29/12 Pct Recovery = 79% Analysis Date = 05/29/12 Pct Recovery = 79% Analysis Date = 05/19/12 Pct Recovery = 79% Analysis Date = 05/19/12 Pct Recovery = 79% Analysis Date = 05/08/12 Pct Recovery = 79% Analysis Date = 05/08/12 Pct Recovery = 79% Analysis Date = 04/27/12 Pct Recovery = 80% Analysis Date = 04/27/12 Pct Recovery = 80% Analysis Date = 04/17/12 Pct Recovery = 80% Analysis Date = 04/17/12 Pct Recovery = 80% Analysis Date = 04/06/12 Pct Recovery = 80% Analysis Date = 04/06/12 Pct Recovery = 80% Analysis Date = 03/26/12 Pct Recovery = 80% Analysis Date = 03/26/12 Pct Recovery = 80% Analysis Date = 03/16/12 Pct Recovery = 81% Analysis Date = 03/16/12 Pct Recovery = 81% Analysis Date = 03/05/12 Pct Recovery = 81% Analysis Date = 03/05/12 Pct Recovery = 81% Analysis Date = 02/23/12 Pct Recovery = 81% Analysis Date = 02/23/12 Pct Recovery = 81% Analysis Date = 02/13/12 Pct Recovery = 81% Analysis Date = 02/13/12 Pct Recovery = 81% Analysis Date = 02/02/12 Pct Recovery = 82% Analysis Date = 02/02/12 Pct Recovery = 82% Analysis Date = 01/22/12 Pct Recovery = 82% Analysis Date = 01/22/12 Pct Recovery = 82% Analysis Date = 01/12/12 Pct Recovery = 82% Analysis Date = 01/12/12 Pct Recovery = 82% Analysis Date = 01/01/12 Pct Recovery = 82% Analysis Date = 01/01/12 Pct Recovery = 82% Analysis Date = 12/21/11 Pct Recovery = 83% Analysis Date = 12/21/11 Pct Recovery = 83% Analysis Date = 12/11/11 Pct Recovery = 83% Analysis Date = 12/11/11 Pct Recovery = 83% Analysis Date = 11/30/11 Pct Recovery = 83% Analysis Date = 11/30/11 Pct Recovery = 83% Analysis Date = 11/19/11 Pct Recovery = 83% Analysis Date = 11/19/11 Pct Recovery = 83% Analysis Date = 11/09/11 Pct Recovery = 84% Analysis Date = 11/09/11 Pct Recovery = 84% Analysis Date = 10/29/11 Pct Recovery = 84% Analysis Date = 10/29/11 Pct Recovery = 84% Analysis Date = 10/18/11 Pct Recovery = 84% Analysis Date = 10/18/11 Pct Recovery = 84% Analysis Date = 10/08/11 Pct Recovery = 84% Analysis Date = 10/08/11 Pct Recovery = 84% Analysis Date = 09/27/11 Pct Recovery = 84% Analysis Date = 09/27/11 Pct Recovery = 84% Analysis Date = 09/16/11 Pct Recovery = 85% Analysis Date = 09/16/11 Pct Recovery = 85% Analysis Date = 09/06/11 Pct Recovery = 85% Analysis Date = 09/06/11 Pct Recovery = 85% Analysis Date = 08/26/11 Pct Recovery = 85% Analysis Date = 08/26/11 Pct Recovery = 85% Analysis Date = 08/15/11 Pct Recovery = 85% Analysis Date = 08/15/11 Pct Recovery = 85% Analysis Date = 08/05/11 Pct Recovery = 85% Analysis Date = 08/05/11 Pct Recovery = 85% Analysis Date = 07/25/11 Pct Recovery = 85% Analysis Date = 07/25/11 Pct Recovery = 85% Analysis Date = 07/14/11 Pct Recovery = 86% Analysis Date = 07/14/11 Pct Recovery = 86% Analysis Date = 07/04/11 Pct Recovery = 86% Analysis Date = 07/04/11 Pct Recovery = 86% Analysis Date = 06/23/11 Pct Recovery = 86% Analysis Date = 06/23/11 Pct Recovery = 86% Analysis Date = 06/12/11 Pct Recovery = 86% Analysis Date = 06/12/11 Pct Recovery = 86% Analysis Date = 06/02/11 Pct Recovery = 86% Analysis Date = 06/02/11 Pct Recovery = 86% Analysis Date = 05/22/11 Pct Recovery = 86% Analysis Date = 05/22/11 Pct Recovery = 86% Analysis Date = 05/11/11 Pct Recovery = 86% Analysis Date = 05/11/11 Pct Recovery = 86% Analysis Date = 05/01/11 Pct Recovery = 87% Analysis Date = 05/01/11 Pct Recovery = 87% Analysis Date = 04/20/11 Pct Recovery = 87% Analysis Date = 04/20/11 Pct Recovery = 87% Analysis Date = 04/09/11 Pct Recovery = 87% Analysis Date = 04/09/11 Pct Recovery = 87% Analysis Date = 03/30/11 Pct Recovery = 87% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
EQUILENIN

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 36 91% 36% 89% 42%
Total 36 91% 36% 89% 42%

Sample Statistics
EQUILENIN

Characteristic N % % Basis
Plotted 36 84% Spiked
Estimated Values 3 7% Spiked
Deleted Values 1 1% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 43 .  
False Negatives 7 16% 7 out of 43
Not Spiked 43 .  
False Positives 8 19% 8 out of 42

BQS OBSP Determination:
EQUILIN
METHOD: 4434 , TESTIDCODE: 64539GM005
Open Data Set

Analysis Date = 12/15/16 SpikeMix = Abs 061416H: 50 µl & ChemService 5016100: 50 µl Pct Recovery = 62% Analysis Date = 08/11/16 SpikeMix = ChemService 5016100: 50 µl & Spex Organics TS160420010: 50 µl Pct Recovery = 82% Analysis Date = 08/19/16 SpikeMix = Supelco LC20140V: 50 µl & Spex Organics TS160420010: 50 µl Pct Recovery = 133% Analysis Date = 12/09/14 SpikeMix = Abs 031014: 60 µl & Supelco LC06946: 60 µl Pct Recovery = 56% Analysis Date = 08/26/14 SpikeMix = Abs 031014: 60 µl & Abs 042114: 60 µl Pct Recovery = 87% Analysis Date = 08/11/14 SpikeMix = Abs 031014: 60 µl & ERA 0227-14-07.2: 60 µl Pct Recovery = 89% Analysis Date = 05/06/14 SpikeMix = Abs 031014: 60 µl & ChemService 2561700: 60 µl Pct Recovery = 45% Analysis Date = 04/13/15 SpikeMix = Abs 042114: 60 µl & Spex Organics E1140505004: 60 µl Pct Recovery = 79% Analysis Date = 04/01/15 SpikeMix = Spex Organics E1140505004: 60 µl & Supelco LC06946: 60 µl Pct Recovery = 54% Analysis Date = 01/21/15 SpikeMix = ChemService 2561700: 60 µl & Spex Organics E1140505004: 60 µl Pct Recovery = 103% Analysis Date = 05/09/11 SpikeMix = Abs 081810: 100 µl Pct Recovery = 65% Analysis Date = 07/02/12 SpikeMix = Abs 081810: 100 µl Pct Recovery = 85% Analysis Date = 04/17/12 SpikeMix = Abs 081810: 100 µl Pct Recovery = 83% Analysis Date = 10/03/11 SpikeMix = Abs 081810: 100 µl Pct Recovery = 79% Analysis Date = 03/14/14 SpikeMix = Supelco LB99393: 50 µl & Abs 050813: 50 µl Pct Recovery = 72% Analysis Date = 02/25/14 SpikeMix = ERA 0415-13-01.1A: 50 µl & Abs 050813: 50 µl Pct Recovery = 53% Analysis Date = 03/14/14 SpikeMix = ERA 0415-13-01.2A: 50 µl & Spex Organics T1130423008: 50 µl Pct Recovery = 51% Analysis Date = 03/05/14 SpikeMix = Spex Organics T1130423008: 50 µl & Abs 071513: 50 µl Pct Recovery = 55% Analysis Date = 08/09/13 SpikeMix = ERA 0415-13-01.2A: 50 µl & Spex Organics T1130423008: 50 µl Pct Recovery = 61% Analysis Date = 01/05/16 SpikeMix = Supelco LC13547: 60 µl & ChemService 4073900: 60 µl Pct Recovery = 77% Analysis Date = 01/07/16 SpikeMix = Crescent 04EE007: 60 µl & Abs 041515: 60 µl Pct Recovery = 73% Analysis Date = 02/22/13 SpikeMix = Restek A089631: 50 µl & Supelco LB92781: 50 µl Pct Recovery = 46% Analysis Date = 12/18/12 SpikeMix = Spex Organics T1120525010: 50 µl & Supelco LB92781: 50 µl Pct Recovery = 66% Analysis Date = 12/03/12 SpikeMix = ERA 0511-12-02: 50 µl & Abs 051512: 50 µl Pct Recovery = 49% Analysis Date = 02/01/12 SpikeMix = Spex Organics T1100629008: 100 µl Pct Recovery = 70% Analysis Date = 03/31/11 SpikeMix = Spex Organics T1100629008: 100 µl Pct Recovery = 76% Analysis Date = 09/21/16 SpikeMix = ChemService 5016200: 30 µl & ChemService 5016100: 30 µl Pct Recovery = 69% Analysis Date = 06/24/16 SpikeMix = ERA 0601-15-04: 50 µl & ChemService 4073900: 50 µl Pct Recovery = 65% Analysis Date = 09/14/15 SpikeMix = ERA 0601-15-04: 50 µl & ChemService 4073900: 50 µl Pct Recovery = 83% Analysis Date = 08/17/15 SpikeMix = ChemService 4073900: 50 µl & Abs 041515: 50 µl Pct Recovery = 75% Analysis Date = 02/01/17 SpikeMix = Supelco LC20140V: 30 µl & Abs 052616: 30 µl Pct Recovery = 63% Analysis Date = 06/24/16 SpikeMix = Crescent 04EE007: 50 µl & Spex Organics EN150501025: 50 µl Pct Recovery = 84% Analysis Date = 01/08/16 SpikeMix = Crescent 04EE007: 50 µl & Spex Organics EN150501025: 50 µl Pct Recovery = 109% Analysis Date = 08/10/15 SpikeMix = ERA 0601-15-04: 50 µl & Crescent 04EE007: 50 µl Pct Recovery = 60% Analysis Date = 06/03/15 SpikeMix = Abs 031014: 30 µl & ERA 0227-14-07.2: 30 µl Pct Recovery = 63% Analysis Date = 01/29/15 SpikeMix = Abs 031014: 30 µl & Supelco LC06946: 30 µl Pct Recovery = 53% Analysis Date = 12/22/14 SpikeMix = Abs 042114: 30 µl & Abs 031014: 30 µl Pct Recovery = 76% Analysis Date = 07/14/14 SpikeMix = ERA 0227-14-07.2: 30 µl & Abs 031014: 30 µl Pct Recovery = 71% Analysis Date = 05/14/14 SpikeMix = Abs 031014: 30 µl & ChemService 2561700: 30 µl Pct Recovery = 71% Analysis Date = 04/01/15 SpikeMix = ChemService 2561700: 30 µl & Spex Organics E1140505004: 30 µl Pct Recovery = 62% Analysis Date = 12/23/14 SpikeMix = Spex Organics E1140505004: 30 µl & Supelco LC06946: 30 µl Pct Recovery = 61% Analysis Date = 01/08/16 SpikeMix = ERA 0601-15-04: 30 µl & ChemService 4073900: 30 µl Pct Recovery = 44% Analysis Date = 09/23/15 SpikeMix = ChemService 4073900: 30 µl & Spex Organics EN150501025: 30 µl Pct Recovery = 103% Analysis Date = 01/08/16 SpikeMix = ERA 0601-15-04: 30 µl & Crescent 04EE007: 30 µl Pct Recovery = 72% Analysis Date = 12/11/15 SpikeMix = Crescent 04EE007: 30 µl & Spex Organics EN150501025: 30 µl Pct Recovery = 80% Analysis Date = 04/10/13 SpikeMix = ERA 0511-12-02: 25 µl & Supelco LB92781: 25 µl Pct Recovery = 89% Analysis Date = 04/03/13 SpikeMix = Spex Organics T1120525010: 25 µl & Abs 051512: 25 µl Pct Recovery = 64% Analysis Date = 02/08/13 SpikeMix = ERA 0507-12-04.1: 25 µl & Supelco LB92781: 25 µl Pct Recovery = 65% Analysis Date = 12/18/12 SpikeMix = Restek A089631: 25 µl & Supelco LB92781: 25 µl Pct Recovery = 73% Analysis Date = 11/01/12 SpikeMix = ERA 0507-12-04.1: 25 µl & Abs 051512: 25 µl Pct Recovery = 64% Analysis Date = 08/31/12 SpikeMix = ERA 0511-12-02: 25 µl & Abs 051512: 25 µl Pct Recovery = 52% Analysis Date = 08/24/12 SpikeMix = Abs 051512: 25 µl Pct Recovery = 59% Analysis Date = 03/03/14 SpikeMix = Abs 050813: 20 µl & Abs 071513: 20 µl Pct Recovery = 40% Analysis Date = 02/19/14 SpikeMix = Abs 050813: 20 µl & Abs 071513: 20 µl Pct Recovery = 51% Analysis Date = 11/18/13 SpikeMix = ERA 0415-13-01.2A: 20 µl & Abs 050813: 20 µl Pct Recovery = 42% Analysis Date = 12/09/13 SpikeMix = Supelco LB99393: 20 µl & Spex Organics T1130423008: 20 µl Pct Recovery = 39% Analysis Date = 06/27/13 SpikeMix = ERA 0415-13-01.1A: 20 µl & Spex Organics T1130423008: 20 µl Pct Recovery = 61% Analysis Date = 06/04/13 SpikeMix = Supelco LB99393: 20 µl & Spex Organics T1130423008: 20 µl Pct Recovery = 62% Analysis Date = 06/13/11 SpikeMix = Abs 081810: 25 µl Pct Recovery = 72% Analysis Date = 05/26/11 SpikeMix = Spex Organics T1100629008: 25 µl Pct Recovery = 78% Analysis Date = 07/11/11 SpikeMix = Spex Organics T1100629008: 25 µl Pct Recovery = 49% Analysis Date = 03/27/12 SpikeMix = Abs 081810: 25 µl Pct Recovery = 64% Analysis Date = 01/27/12 SpikeMix = Abs 081810: 25 µl Pct Recovery = 58% Analysis Date = 10/12/11 SpikeMix = Abs 081810: 25 µl Pct Recovery = 64% Analysis Date = 08/16/12 SpikeMix = Spex Organics T1100629008: 25 µl Pct Recovery = 66% Analysis Date = 10/13/11 SpikeMix = Spex Organics T1100629008: 25 µl Pct Recovery = 104% Analysis Date = 01/31/17 Pct Recovery = 80% Analysis Date = 01/21/17 Pct Recovery = 80% Analysis Date = 01/21/17 Pct Recovery = 80% Analysis Date = 01/10/17 Pct Recovery = 80% Analysis Date = 01/10/17 Pct Recovery = 80% Analysis Date = 12/30/16 Pct Recovery = 80% Analysis Date = 12/30/16 Pct Recovery = 80% Analysis Date = 12/20/16 Pct Recovery = 80% Analysis Date = 12/20/16 Pct Recovery = 80% Analysis Date = 12/09/16 Pct Recovery = 80% Analysis Date = 12/09/16 Pct Recovery = 80% Analysis Date = 11/28/16 Pct Recovery = 80% Analysis Date = 11/28/16 Pct Recovery = 80% Analysis Date = 11/18/16 Pct Recovery = 80% Analysis Date = 11/18/16 Pct Recovery = 80% Analysis Date = 11/07/16 Pct Recovery = 80% Analysis Date = 11/07/16 Pct Recovery = 80% Analysis Date = 10/27/16 Pct Recovery = 79% Analysis Date = 10/27/16 Pct Recovery = 79% Analysis Date = 10/17/16 Pct Recovery = 79% Analysis Date = 10/17/16 Pct Recovery = 79% Analysis Date = 10/06/16 Pct Recovery = 79% Analysis Date = 10/06/16 Pct Recovery = 79% Analysis Date = 09/25/16 Pct Recovery = 79% Analysis Date = 09/25/16 Pct Recovery = 79% Analysis Date = 09/15/16 Pct Recovery = 79% Analysis Date = 09/15/16 Pct Recovery = 79% Analysis Date = 09/04/16 Pct Recovery = 79% Analysis Date = 09/04/16 Pct Recovery = 79% Analysis Date = 08/24/16 Pct Recovery = 79% Analysis Date = 08/24/16 Pct Recovery = 79% Analysis Date = 08/14/16 Pct Recovery = 79% Analysis Date = 08/14/16 Pct Recovery = 79% Analysis Date = 08/03/16 Pct Recovery = 79% Analysis Date = 08/03/16 Pct Recovery = 79% Analysis Date = 07/23/16 Pct Recovery = 79% Analysis Date = 07/23/16 Pct Recovery = 79% Analysis Date = 07/13/16 Pct Recovery = 78% Analysis Date = 07/13/16 Pct Recovery = 78% Analysis Date = 07/02/16 Pct Recovery = 78% Analysis Date = 07/02/16 Pct Recovery = 78% Analysis Date = 06/21/16 Pct Recovery = 78% Analysis Date = 06/21/16 Pct Recovery = 78% Analysis Date = 06/11/16 Pct Recovery = 78% Analysis Date = 06/11/16 Pct Recovery = 78% Analysis Date = 05/31/16 Pct Recovery = 78% Analysis Date = 05/31/16 Pct Recovery = 78% Analysis Date = 05/20/16 Pct Recovery = 78% Analysis Date = 05/20/16 Pct Recovery = 78% Analysis Date = 05/10/16 Pct Recovery = 78% Analysis Date = 05/10/16 Pct Recovery = 78% Analysis Date = 04/29/16 Pct Recovery = 78% Analysis Date = 04/29/16 Pct Recovery = 78% Analysis Date = 04/18/16 Pct Recovery = 78% Analysis Date = 04/18/16 Pct Recovery = 78% Analysis Date = 04/08/16 Pct Recovery = 77% Analysis Date = 04/08/16 Pct Recovery = 77% Analysis Date = 03/28/16 Pct Recovery = 77% Analysis Date = 03/28/16 Pct Recovery = 77% Analysis Date = 03/17/16 Pct Recovery = 77% Analysis Date = 03/17/16 Pct Recovery = 77% Analysis Date = 03/07/16 Pct Recovery = 77% Analysis Date = 03/07/16 Pct Recovery = 77% Analysis Date = 02/25/16 Pct Recovery = 77% Analysis Date = 02/25/16 Pct Recovery = 77% Analysis Date = 02/14/16 Pct Recovery = 77% Analysis Date = 02/14/16 Pct Recovery = 77% Analysis Date = 02/04/16 Pct Recovery = 77% Analysis Date = 02/04/16 Pct Recovery = 77% Analysis Date = 01/24/16 Pct Recovery = 77% Analysis Date = 01/24/16 Pct Recovery = 77% Analysis Date = 01/13/16 Pct Recovery = 77% Analysis Date = 01/13/16 Pct Recovery = 77% Analysis Date = 01/03/16 Pct Recovery = 76% Analysis Date = 01/03/16 Pct Recovery = 76% Analysis Date = 12/23/15 Pct Recovery = 76% Analysis Date = 12/23/15 Pct Recovery = 76% Analysis Date = 12/12/15 Pct Recovery = 76% Analysis Date = 12/12/15 Pct Recovery = 76% Analysis Date = 12/02/15 Pct Recovery = 76% Analysis Date = 12/02/15 Pct Recovery = 76% Analysis Date = 11/21/15 Pct Recovery = 76% Analysis Date = 11/21/15 Pct Recovery = 76% Analysis Date = 11/10/15 Pct Recovery = 76% Analysis Date = 11/10/15 Pct Recovery = 76% Analysis Date = 10/31/15 Pct Recovery = 76% Analysis Date = 10/31/15 Pct Recovery = 76% Analysis Date = 10/20/15 Pct Recovery = 76% Analysis Date = 10/20/15 Pct Recovery = 76% Analysis Date = 10/09/15 Pct Recovery = 75% Analysis Date = 10/09/15 Pct Recovery = 75% Analysis Date = 09/29/15 Pct Recovery = 75% Analysis Date = 09/29/15 Pct Recovery = 75% Analysis Date = 09/18/15 Pct Recovery = 75% Analysis Date = 09/18/15 Pct Recovery = 75% Analysis Date = 09/07/15 Pct Recovery = 75% Analysis Date = 09/07/15 Pct Recovery = 75% Analysis Date = 08/28/15 Pct Recovery = 75% Analysis Date = 08/28/15 Pct Recovery = 75% Analysis Date = 08/17/15 Pct Recovery = 75% Analysis Date = 08/17/15 Pct Recovery = 75% Analysis Date = 08/06/15 Pct Recovery = 75% Analysis Date = 08/06/15 Pct Recovery = 75% Analysis Date = 07/27/15 Pct Recovery = 74% Analysis Date = 07/27/15 Pct Recovery = 74% Analysis Date = 07/16/15 Pct Recovery = 74% Analysis Date = 07/16/15 Pct Recovery = 74% Analysis Date = 07/05/15 Pct Recovery = 74% Analysis Date = 07/05/15 Pct Recovery = 74% Analysis Date = 06/25/15 Pct Recovery = 73% Analysis Date = 06/25/15 Pct Recovery = 73% Analysis Date = 06/14/15 Pct Recovery = 73% Analysis Date = 06/14/15 Pct Recovery = 73% Analysis Date = 06/03/15 Pct Recovery = 73% Analysis Date = 06/03/15 Pct Recovery = 73% Analysis Date = 05/24/15 Pct Recovery = 73% Analysis Date = 05/24/15 Pct Recovery = 73% Analysis Date = 05/13/15 Pct Recovery = 72% Analysis Date = 05/13/15 Pct Recovery = 72% Analysis Date = 05/02/15 Pct Recovery = 72% Analysis Date = 05/02/15 Pct Recovery = 72% Analysis Date = 04/22/15 Pct Recovery = 72% Analysis Date = 04/22/15 Pct Recovery = 72% Analysis Date = 04/11/15 Pct Recovery = 71% Analysis Date = 04/11/15 Pct Recovery = 71% Analysis Date = 03/31/15 Pct Recovery = 71% Analysis Date = 03/31/15 Pct Recovery = 71% Analysis Date = 03/21/15 Pct Recovery = 71% Analysis Date = 03/21/15 Pct Recovery = 71% Analysis Date = 03/10/15 Pct Recovery = 70% Analysis Date = 03/10/15 Pct Recovery = 70% Analysis Date = 02/27/15 Pct Recovery = 70% Analysis Date = 02/27/15 Pct Recovery = 70% Analysis Date = 02/17/15 Pct Recovery = 70% Analysis Date = 02/17/15 Pct Recovery = 70% Analysis Date = 02/06/15 Pct Recovery = 69% Analysis Date = 02/06/15 Pct Recovery = 69% Analysis Date = 01/26/15 Pct Recovery = 69% Analysis Date = 01/26/15 Pct Recovery = 69% Analysis Date = 01/16/15 Pct Recovery = 69% Analysis Date = 01/16/15 Pct Recovery = 69% Analysis Date = 01/05/15 Pct Recovery = 68% Analysis Date = 01/05/15 Pct Recovery = 68% Analysis Date = 12/25/14 Pct Recovery = 68% Analysis Date = 12/25/14 Pct Recovery = 68% Analysis Date = 12/15/14 Pct Recovery = 68% Analysis Date = 12/15/14 Pct Recovery = 68% Analysis Date = 12/04/14 Pct Recovery = 67% Analysis Date = 12/04/14 Pct Recovery = 67% Analysis Date = 11/23/14 Pct Recovery = 67% Analysis Date = 11/23/14 Pct Recovery = 67% Analysis Date = 11/13/14 Pct Recovery = 67% Analysis Date = 11/13/14 Pct Recovery = 67% Analysis Date = 11/02/14 Pct Recovery = 66% Analysis Date = 11/02/14 Pct Recovery = 66% Analysis Date = 10/22/14 Pct Recovery = 66% Analysis Date = 10/22/14 Pct Recovery = 66% Analysis Date = 10/12/14 Pct Recovery = 66% Analysis Date = 10/12/14 Pct Recovery = 66% Analysis Date = 10/01/14 Pct Recovery = 65% Analysis Date = 10/01/14 Pct Recovery = 65% Analysis Date = 09/20/14 Pct Recovery = 65% Analysis Date = 09/20/14 Pct Recovery = 65% Analysis Date = 09/10/14 Pct Recovery = 65% Analysis Date = 09/10/14 Pct Recovery = 65% Analysis Date = 08/30/14 Pct Recovery = 64% Analysis Date = 08/30/14 Pct Recovery = 64% Analysis Date = 08/19/14 Pct Recovery = 64% Analysis Date = 08/19/14 Pct Recovery = 64% Analysis Date = 08/09/14 Pct Recovery = 63% Analysis Date = 08/09/14 Pct Recovery = 63% Analysis Date = 07/29/14 Pct Recovery = 63% Analysis Date = 07/29/14 Pct Recovery = 63% Analysis Date = 07/18/14 Pct Recovery = 63% Analysis Date = 07/18/14 Pct Recovery = 63% Analysis Date = 07/08/14 Pct Recovery = 63% Analysis Date = 07/08/14 Pct Recovery = 63% Analysis Date = 06/27/14 Pct Recovery = 62% Analysis Date = 06/27/14 Pct Recovery = 62% Analysis Date = 06/16/14 Pct Recovery = 62% Analysis Date = 06/16/14 Pct Recovery = 62% Analysis Date = 06/06/14 Pct Recovery = 62% Analysis Date = 06/06/14 Pct Recovery = 62% Analysis Date = 05/26/14 Pct Recovery = 62% Analysis Date = 05/26/14 Pct Recovery = 62% Analysis Date = 05/15/14 Pct Recovery = 62% Analysis Date = 05/15/14 Pct Recovery = 62% Analysis Date = 05/05/14 Pct Recovery = 62% Analysis Date = 05/05/14 Pct Recovery = 62% Analysis Date = 04/24/14 Pct Recovery = 62% Analysis Date = 04/24/14 Pct Recovery = 62% Analysis Date = 04/13/14 Pct Recovery = 62% Analysis Date = 04/13/14 Pct Recovery = 62% Analysis Date = 04/03/14 Pct Recovery = 62% Analysis Date = 04/03/14 Pct Recovery = 62% Analysis Date = 03/23/14 Pct Recovery = 61% Analysis Date = 03/23/14 Pct Recovery = 61% Analysis Date = 03/12/14 Pct Recovery = 61% Analysis Date = 03/12/14 Pct Recovery = 61% Analysis Date = 03/01/14 Pct Recovery = 61% Analysis Date = 03/01/14 Pct Recovery = 61% Analysis Date = 02/19/14 Pct Recovery = 61% Analysis Date = 02/19/14 Pct Recovery = 61% Analysis Date = 02/08/14 Pct Recovery = 61% Analysis Date = 02/08/14 Pct Recovery = 61% Analysis Date = 01/28/14 Pct Recovery = 61% Analysis Date = 01/28/14 Pct Recovery = 61% Analysis Date = 01/18/14 Pct Recovery = 61% Analysis Date = 01/18/14 Pct Recovery = 61% Analysis Date = 01/07/14 Pct Recovery = 61% Analysis Date = 01/07/14 Pct Recovery = 61% Analysis Date = 12/27/13 Pct Recovery = 61% Analysis Date = 12/27/13 Pct Recovery = 61% Analysis Date = 12/17/13 Pct Recovery = 61% Analysis Date = 12/17/13 Pct Recovery = 61% Analysis Date = 12/06/13 Pct Recovery = 61% Analysis Date = 12/06/13 Pct Recovery = 61% Analysis Date = 11/25/13 Pct Recovery = 61% Analysis Date = 11/25/13 Pct Recovery = 61% Analysis Date = 11/15/13 Pct Recovery = 61% Analysis Date = 11/15/13 Pct Recovery = 61% Analysis Date = 11/04/13 Pct Recovery = 61% Analysis Date = 11/04/13 Pct Recovery = 61% Analysis Date = 10/24/13 Pct Recovery = 61% Analysis Date = 10/24/13 Pct Recovery = 61% Analysis Date = 10/14/13 Pct Recovery = 61% Analysis Date = 10/14/13 Pct Recovery = 61% Analysis Date = 10/03/13 Pct Recovery = 61% Analysis Date = 10/03/13 Pct Recovery = 61% Analysis Date = 09/22/13 Pct Recovery = 61% Analysis Date = 09/22/13 Pct Recovery = 61% Analysis Date = 09/12/13 Pct Recovery = 61% Analysis Date = 09/12/13 Pct Recovery = 61% Analysis Date = 09/01/13 Pct Recovery = 61% Analysis Date = 09/01/13 Pct Recovery = 61% Analysis Date = 08/21/13 Pct Recovery = 61% Analysis Date = 08/21/13 Pct Recovery = 61% Analysis Date = 08/11/13 Pct Recovery = 61% Analysis Date = 08/11/13 Pct Recovery = 61% Analysis Date = 07/31/13 Pct Recovery = 61% Analysis Date = 07/31/13 Pct Recovery = 61% Analysis Date = 07/20/13 Pct Recovery = 61% Analysis Date = 07/20/13 Pct Recovery = 61% Analysis Date = 07/10/13 Pct Recovery = 61% Analysis Date = 07/10/13 Pct Recovery = 61% Analysis Date = 06/29/13 Pct Recovery = 61% Analysis Date = 06/29/13 Pct Recovery = 61% Analysis Date = 06/18/13 Pct Recovery = 61% Analysis Date = 06/18/13 Pct Recovery = 61% Analysis Date = 06/08/13 Pct Recovery = 61% Analysis Date = 06/08/13 Pct Recovery = 61% Analysis Date = 05/28/13 Pct Recovery = 61% Analysis Date = 05/28/13 Pct Recovery = 61% Analysis Date = 05/17/13 Pct Recovery = 61% Analysis Date = 05/17/13 Pct Recovery = 61% Analysis Date = 05/07/13 Pct Recovery = 61% Analysis Date = 05/07/13 Pct Recovery = 61% Analysis Date = 04/26/13 Pct Recovery = 61% Analysis Date = 04/26/13 Pct Recovery = 61% Analysis Date = 04/15/13 Pct Recovery = 62% Analysis Date = 04/15/13 Pct Recovery = 62% Analysis Date = 04/05/13 Pct Recovery = 62% Analysis Date = 04/05/13 Pct Recovery = 62% Analysis Date = 03/25/13 Pct Recovery = 62% Analysis Date = 03/25/13 Pct Recovery = 62% Analysis Date = 03/14/13 Pct Recovery = 62% Analysis Date = 03/14/13 Pct Recovery = 62% Analysis Date = 03/04/13 Pct Recovery = 62% Analysis Date = 03/04/13 Pct Recovery = 62% Analysis Date = 02/21/13 Pct Recovery = 62% Analysis Date = 02/21/13 Pct Recovery = 62% Analysis Date = 02/10/13 Pct Recovery = 63% Analysis Date = 02/10/13 Pct Recovery = 63% Analysis Date = 01/31/13 Pct Recovery = 63% Analysis Date = 01/31/13 Pct Recovery = 63% Analysis Date = 01/20/13 Pct Recovery = 63% Analysis Date = 01/20/13 Pct Recovery = 63% Analysis Date = 01/09/13 Pct Recovery = 63% Analysis Date = 01/09/13 Pct Recovery = 63% Analysis Date = 12/30/12 Pct Recovery = 64% Analysis Date = 12/30/12 Pct Recovery = 64% Analysis Date = 12/19/12 Pct Recovery = 64% Analysis Date = 12/19/12 Pct Recovery = 64% Analysis Date = 12/08/12 Pct Recovery = 64% Analysis Date = 12/08/12 Pct Recovery = 64% Analysis Date = 11/28/12 Pct Recovery = 64% Analysis Date = 11/28/12 Pct Recovery = 64% Analysis Date = 11/17/12 Pct Recovery = 65% Analysis Date = 11/17/12 Pct Recovery = 65% Analysis Date = 11/06/12 Pct Recovery = 65% Analysis Date = 11/06/12 Pct Recovery = 65% Analysis Date = 10/27/12 Pct Recovery = 65% Analysis Date = 10/27/12 Pct Recovery = 65% Analysis Date = 10/16/12 Pct Recovery = 65% Analysis Date = 10/16/12 Pct Recovery = 65% Analysis Date = 10/05/12 Pct Recovery = 65% Analysis Date = 10/05/12 Pct Recovery = 65% Analysis Date = 09/25/12 Pct Recovery = 66% Analysis Date = 09/25/12 Pct Recovery = 66% Analysis Date = 09/14/12 Pct Recovery = 66% Analysis Date = 09/14/12 Pct Recovery = 66% Analysis Date = 09/03/12 Pct Recovery = 66% Analysis Date = 09/03/12 Pct Recovery = 66% Analysis Date = 08/24/12 Pct Recovery = 66% Analysis Date = 08/24/12 Pct Recovery = 66% Analysis Date = 08/13/12 Pct Recovery = 66% Analysis Date = 08/13/12 Pct Recovery = 66% Analysis Date = 08/02/12 Pct Recovery = 66% Analysis Date = 08/02/12 Pct Recovery = 66% Analysis Date = 07/23/12 Pct Recovery = 67% Analysis Date = 07/23/12 Pct Recovery = 67% Analysis Date = 07/12/12 Pct Recovery = 67% Analysis Date = 07/12/12 Pct Recovery = 67% Analysis Date = 07/01/12 Pct Recovery = 67% Analysis Date = 07/01/12 Pct Recovery = 67% Analysis Date = 06/21/12 Pct Recovery = 67% Analysis Date = 06/21/12 Pct Recovery = 67% Analysis Date = 06/10/12 Pct Recovery = 67% Analysis Date = 06/10/12 Pct Recovery = 67% Analysis Date = 05/30/12 Pct Recovery = 68% Analysis Date = 05/30/12 Pct Recovery = 68% Analysis Date = 05/20/12 Pct Recovery = 68% Analysis Date = 05/20/12 Pct Recovery = 68% Analysis Date = 05/09/12 Pct Recovery = 68% Analysis Date = 05/09/12 Pct Recovery = 68% Analysis Date = 04/28/12 Pct Recovery = 68% Analysis Date = 04/28/12 Pct Recovery = 68% Analysis Date = 04/18/12 Pct Recovery = 68% Analysis Date = 04/18/12 Pct Recovery = 68% Analysis Date = 04/07/12 Pct Recovery = 68% Analysis Date = 04/07/12 Pct Recovery = 68% Analysis Date = 03/27/12 Pct Recovery = 69% Analysis Date = 03/27/12 Pct Recovery = 69% Analysis Date = 03/17/12 Pct Recovery = 69% Analysis Date = 03/17/12 Pct Recovery = 69% Analysis Date = 03/06/12 Pct Recovery = 69% Analysis Date = 03/06/12 Pct Recovery = 69% Analysis Date = 02/24/12 Pct Recovery = 69% Analysis Date = 02/24/12 Pct Recovery = 69% Analysis Date = 02/14/12 Pct Recovery = 69% Analysis Date = 02/14/12 Pct Recovery = 69% Analysis Date = 02/03/12 Pct Recovery = 69% Analysis Date = 02/03/12 Pct Recovery = 69% Analysis Date = 01/23/12 Pct Recovery = 70% Analysis Date = 01/23/12 Pct Recovery = 70% Analysis Date = 01/13/12 Pct Recovery = 70% Analysis Date = 01/13/12 Pct Recovery = 70% Analysis Date = 01/02/12 Pct Recovery = 70% Analysis Date = 01/02/12 Pct Recovery = 70% Analysis Date = 12/22/11 Pct Recovery = 70% Analysis Date = 12/22/11 Pct Recovery = 70% Analysis Date = 12/12/11 Pct Recovery = 70% Analysis Date = 12/12/11 Pct Recovery = 70% Analysis Date = 12/01/11 Pct Recovery = 70% Analysis Date = 12/01/11 Pct Recovery = 70% Analysis Date = 11/20/11 Pct Recovery = 71% Analysis Date = 11/20/11 Pct Recovery = 71% Analysis Date = 11/10/11 Pct Recovery = 71% Analysis Date = 11/10/11 Pct Recovery = 71% Analysis Date = 10/30/11 Pct Recovery = 71% Analysis Date = 10/30/11 Pct Recovery = 71% Analysis Date = 10/19/11 Pct Recovery = 71% Analysis Date = 10/19/11 Pct Recovery = 71% Analysis Date = 10/09/11 Pct Recovery = 71% Analysis Date = 10/09/11 Pct Recovery = 71% Analysis Date = 09/28/11 Pct Recovery = 72% Analysis Date = 09/28/11 Pct Recovery = 72% Analysis Date = 09/17/11 Pct Recovery = 72% Analysis Date = 09/17/11 Pct Recovery = 72% Analysis Date = 09/07/11 Pct Recovery = 72% Analysis Date = 09/07/11 Pct Recovery = 72% Analysis Date = 08/27/11 Pct Recovery = 72% Analysis Date = 08/27/11 Pct Recovery = 72% Analysis Date = 08/16/11 Pct Recovery = 72% Analysis Date = 08/16/11 Pct Recovery = 72% Analysis Date = 08/06/11 Pct Recovery = 72% Analysis Date = 08/06/11 Pct Recovery = 72% Analysis Date = 07/26/11 Pct Recovery = 73% Analysis Date = 07/26/11 Pct Recovery = 73% Analysis Date = 07/15/11 Pct Recovery = 73% Analysis Date = 07/15/11 Pct Recovery = 73% Analysis Date = 07/05/11 Pct Recovery = 73% Analysis Date = 07/05/11 Pct Recovery = 73% Analysis Date = 06/24/11 Pct Recovery = 73% Analysis Date = 06/24/11 Pct Recovery = 73% Analysis Date = 06/13/11 Pct Recovery = 73% Analysis Date = 06/13/11 Pct Recovery = 73% Analysis Date = 06/03/11 Pct Recovery = 73% Analysis Date = 06/03/11 Pct Recovery = 73% Analysis Date = 05/23/11 Pct Recovery = 74% Analysis Date = 05/23/11 Pct Recovery = 74% Analysis Date = 05/12/11 Pct Recovery = 74% Analysis Date = 05/12/11 Pct Recovery = 74% Analysis Date = 05/02/11 Pct Recovery = 74% Analysis Date = 05/02/11 Pct Recovery = 74% Analysis Date = 04/21/11 Pct Recovery = 74% Analysis Date = 04/21/11 Pct Recovery = 74% Analysis Date = 04/10/11 Pct Recovery = 74% Analysis Date = 04/10/11 Pct Recovery = 74% Analysis Date = 03/31/11 Pct Recovery = 74% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
EQUILIN

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 5 71% 18% 64% 1%
>= Reporting Level 61 68% 18% 65% 16%
Total 66 69% 18% 65% 14%

Sample Statistics
EQUILIN

Characteristic N % % Basis
Plotted 66 85% Spiked
Estimated Values 66 85% Spiked
Deleted Values 2 2% Spiked + Not Spiked
Spiked, Censored 1 1% Spiked
Spiked 79 .  
False Negatives 11 14% 11 out of 78
Not Spiked 52 .  
False Positives 0 0% 0 out of 51

BQS OBSP Determination:
ESTRIOL
METHOD: 4434 , TESTIDCODE: 64540GM005
Open Data Set

Analysis Date = 05/09/11 SpikeMix = Abs 081810: 100 µl Pct Recovery = 83% Analysis Date = 02/22/13 SpikeMix = Restek A089631: 50 µl & Supelco LB92781: 50 µl Pct Recovery = 76% Analysis Date = 12/18/12 SpikeMix = Spex Organics T1120525010: 50 µl & Supelco LB92781: 50 µl Pct Recovery = 76% Analysis Date = 07/02/12 SpikeMix = Abs 081810: 100 µl Pct Recovery = 103% Analysis Date = 04/17/12 SpikeMix = Abs 081810: 100 µl Pct Recovery = 94% Analysis Date = 02/01/12 SpikeMix = Spex Organics T1100629008: 100 µl Pct Recovery = 79% Analysis Date = 10/03/11 SpikeMix = Abs 081810: 100 µl Pct Recovery = 91% Analysis Date = 09/29/11 SpikeMix = Spex Organics T1100629008: 100 µl Pct Recovery = 75% Analysis Date = 03/31/11 SpikeMix = Spex Organics T1100629008: 100 µl Pct Recovery = 87% Analysis Date = 12/03/12 SpikeMix = ERA 0511-12-02: 50 µl & Abs 051512: 50 µl Pct Recovery = 65% Analysis Date = 03/14/14 SpikeMix = Supelco LB99393: 50 µl & Abs 050813: 50 µl Pct Recovery = 68% Analysis Date = 02/25/14 SpikeMix = ERA 0415-13-01.1A: 50 µl & Abs 050813: 50 µl Pct Recovery = 73% Analysis Date = 03/14/14 SpikeMix = ERA 0415-13-01.2A: 50 µl & Spex Organics T1130423008: 50 µl Pct Recovery = 59% Analysis Date = 03/05/14 SpikeMix = Spex Organics T1130423008: 50 µl & Abs 071513: 50 µl Pct Recovery = 63% Analysis Date = 08/09/13 SpikeMix = ERA 0415-13-01.2A: 50 µl & Spex Organics T1130423008: 50 µl Pct Recovery = 92% Analysis Date = 04/10/13 SpikeMix = ERA 0511-12-02: 25 µl & Supelco LB92781: 25 µl Pct Recovery = 81% Analysis Date = 02/08/13 SpikeMix = ERA 0507-12-04.1: 25 µl & Supelco LB92781: 25 µl Pct Recovery = 81% Analysis Date = 12/18/12 SpikeMix = Restek A089631: 25 µl & Supelco LB92781: 25 µl Pct Recovery = 71% Analysis Date = 04/03/13 SpikeMix = Spex Organics T1120525010: 25 µl & Abs 051512: 25 µl Pct Recovery = 61% Analysis Date = 11/01/12 SpikeMix = ERA 0507-12-04.1: 25 µl & Abs 051512: 25 µl Pct Recovery = 72% Analysis Date = 08/31/12 SpikeMix = ERA 0511-12-02: 25 µl & Abs 051512: 25 µl Pct Recovery = 91% Analysis Date = 08/24/12 SpikeMix = Abs 051512: 25 µl Pct Recovery = 83% Analysis Date = 12/15/16 SpikeMix = Abs 061416H: 50 µl & ChemService 5016100: 50 µl Pct Recovery = 88% Analysis Date = 04/01/15 SpikeMix = ERA 0227-14-07.2: 60 µl & ChemService 2561700: 60 µl Pct Recovery = 81% Analysis Date = 04/01/15 SpikeMix = Spex Organics E1140505004: 60 µl & Supelco LC06946: 60 µl Pct Recovery = 81% Analysis Date = 02/12/15 SpikeMix = Supelco LC06946: 60 µl & Abs 042114: 60 µl Pct Recovery = 88% Analysis Date = 12/09/14 SpikeMix = Abs 031014: 60 µl & Supelco LC06946: 60 µl Pct Recovery = 58% Analysis Date = 09/23/14 SpikeMix = Supelco LC06946: 60 µl & ChemService 2561700: 60 µl Pct Recovery = 89% Analysis Date = 01/05/16 SpikeMix = Supelco LC13547: 60 µl & ChemService 4073900: 60 µl Pct Recovery = 77% Analysis Date = 01/07/16 SpikeMix = Crescent 04EE007: 60 µl & Abs 041515: 60 µl Pct Recovery = 79% Analysis Date = 05/26/11 SpikeMix = Spex Organics T1100629008: 25 µl Pct Recovery = 78% Analysis Date = 08/16/12 SpikeMix = Spex Organics T1100629008: 25 µl Pct Recovery = 74% Analysis Date = 03/27/12 SpikeMix = Abs 081810: 25 µl Pct Recovery = 98% Analysis Date = 01/27/12 SpikeMix = Abs 081810: 25 µl Pct Recovery = 84% Analysis Date = 11/28/11 SpikeMix = Spex Organics T1100629008: 25 µl Pct Recovery = 88% Analysis Date = 10/13/11 SpikeMix = Spex Organics T1100629008: 25 µl Pct Recovery = 80% Analysis Date = 10/12/11 SpikeMix = Abs 081810: 25 µl Pct Recovery = 78% Analysis Date = 03/10/11 SpikeMix = Spex Organics T1100629008: 25 µl Pct Recovery = 59% Analysis Date = 07/11/11 SpikeMix = Spex Organics T1100629008: 25 µl Pct Recovery = 52% Analysis Date = 06/13/11 SpikeMix = Abs 081810: 25 µl Pct Recovery = 59% Analysis Date = 03/30/11 SpikeMix = Abs 081810: 25 µl Pct Recovery = 115% Analysis Date = 03/03/14 SpikeMix = Abs 050813: 20 µl & Abs 071513: 20 µl Pct Recovery = 58% Analysis Date = 02/19/14 SpikeMix = Abs 050813: 20 µl & Abs 071513: 20 µl Pct Recovery = 69% Analysis Date = 11/18/13 SpikeMix = ERA 0415-13-01.2A: 20 µl & Abs 050813: 20 µl Pct Recovery = 62% Analysis Date = 12/09/13 SpikeMix = Supelco LB99393: 20 µl & Spex Organics T1130423008: 20 µl Pct Recovery = 68% Analysis Date = 06/27/13 SpikeMix = ERA 0415-13-01.1A: 20 µl & Spex Organics T1130423008: 20 µl Pct Recovery = 48% Analysis Date = 06/04/13 SpikeMix = Supelco LB99393: 20 µl & Spex Organics T1130423008: 20 µl Pct Recovery = 64% Analysis Date = 01/13/17 SpikeMix = Abs 052616: 30 µl & ChemService 5016200: 30 µl Pct Recovery = 80% Analysis Date = 09/21/16 SpikeMix = ChemService 5016200: 30 µl & ChemService 5016100: 30 µl Pct Recovery = 106% Analysis Date = 09/16/16 SpikeMix = Spex Organics EN160621015: 30 µl & ChemService 5016200: 30 µl Pct Recovery = 98% Analysis Date = 09/09/16 SpikeMix = ChemService 5016200: 30 µl & Supelco LC20140V: 30 µl Pct Recovery = 92% Analysis Date = 06/24/16 SpikeMix = ERA 0601-15-04: 50 µl & ChemService 4073900: 50 µl Pct Recovery = 88% Analysis Date = 09/14/15 SpikeMix = ERA 0601-15-04: 50 µl & ChemService 4073900: 50 µl Pct Recovery = 93% Analysis Date = 08/17/15 SpikeMix = ChemService 4073900: 50 µl & Abs 041515: 50 µl Pct Recovery = 107% Analysis Date = 12/05/16 SpikeMix = Abs 052616: 30 µl & Abs 061416H: 30 µl Pct Recovery = 104% Analysis Date = 06/24/16 SpikeMix = Crescent 04EE007: 50 µl & Spex Organics EN150501025: 50 µl Pct Recovery = 85% Analysis Date = 01/08/16 SpikeMix = Crescent 04EE007: 50 µl & Spex Organics EN150501025: 50 µl Pct Recovery = 115% Analysis Date = 08/10/15 SpikeMix = ERA 0601-15-04: 50 µl & Crescent 04EE007: 50 µl Pct Recovery = 81% Analysis Date = 11/05/14 SpikeMix = ERA 0227-14-07.2: 30 µl & Abs 042114: 30 µl Pct Recovery = 91% Analysis Date = 09/04/14 SpikeMix = ERA 0227-14-07.2: 30 µl & Spex Organics E1140505004: 30 µl Pct Recovery = 91% Analysis Date = 07/28/14 SpikeMix = ERA 0227-14-07.2: 30 µl & ChemService 2561700: 30 µl Pct Recovery = 93% Analysis Date = 07/14/14 SpikeMix = ERA 0227-14-07.2: 30 µl & Abs 031014: 30 µl Pct Recovery = 79% Analysis Date = 01/29/15 SpikeMix = Abs 031014: 30 µl & Supelco LC06946: 30 µl Pct Recovery = 64% Analysis Date = 01/21/15 SpikeMix = Supelco LC06946: 30 µl & ChemService 2561700: 30 µl Pct Recovery = 98% Analysis Date = 12/23/14 SpikeMix = Spex Organics E1140505004: 30 µl & Supelco LC06946: 30 µl Pct Recovery = 81% Analysis Date = 12/16/14 SpikeMix = Supelco LC06946: 30 µl & Abs 042114: 30 µl Pct Recovery = 88% Analysis Date = 03/18/16 SpikeMix = Supelco LC13547: 30 µl & ChemService 4073900: 30 µl Pct Recovery = 105% Analysis Date = 03/07/16 SpikeMix = ChemService 4073900: 30 µl & Abs 041515: 30 µl Pct Recovery = 52% Analysis Date = 01/08/16 SpikeMix = ERA 0601-15-04: 30 µl & ChemService 4073900: 30 µl Pct Recovery = 89% Analysis Date = 09/23/15 SpikeMix = ChemService 4073900: 30 µl & Spex Organics EN150501025: 30 µl Pct Recovery = 121% Analysis Date = 03/18/16 SpikeMix = Crescent 04EE007: 30 µl & Spex Organics EN150501025: 30 µl Pct Recovery = 110% Analysis Date = 01/08/16 SpikeMix = ERA 0601-15-04: 30 µl & Crescent 04EE007: 30 µl Pct Recovery = 71% Analysis Date = 01/13/17 Pct Recovery = 95% Analysis Date = 01/02/17 Pct Recovery = 95% Analysis Date = 01/02/17 Pct Recovery = 95% Analysis Date = 12/22/16 Pct Recovery = 95% Analysis Date = 12/22/16 Pct Recovery = 95% Analysis Date = 12/11/16 Pct Recovery = 95% Analysis Date = 12/11/16 Pct Recovery = 95% Analysis Date = 12/01/16 Pct Recovery = 94% Analysis Date = 12/01/16 Pct Recovery = 94% Analysis Date = 11/20/16 Pct Recovery = 94% Analysis Date = 11/20/16 Pct Recovery = 94% Analysis Date = 11/09/16 Pct Recovery = 94% Analysis Date = 11/09/16 Pct Recovery = 94% Analysis Date = 10/30/16 Pct Recovery = 94% Analysis Date = 10/30/16 Pct Recovery = 94% Analysis Date = 10/19/16 Pct Recovery = 94% Analysis Date = 10/19/16 Pct Recovery = 94% Analysis Date = 10/08/16 Pct Recovery = 94% Analysis Date = 10/08/16 Pct Recovery = 94% Analysis Date = 09/28/16 Pct Recovery = 94% Analysis Date = 09/28/16 Pct Recovery = 94% Analysis Date = 09/17/16 Pct Recovery = 93% Analysis Date = 09/17/16 Pct Recovery = 93% Analysis Date = 09/06/16 Pct Recovery = 93% Analysis Date = 09/06/16 Pct Recovery = 93% Analysis Date = 08/27/16 Pct Recovery = 93% Analysis Date = 08/27/16 Pct Recovery = 93% Analysis Date = 08/16/16 Pct Recovery = 93% Analysis Date = 08/16/16 Pct Recovery = 93% Analysis Date = 08/05/16 Pct Recovery = 93% Analysis Date = 08/05/16 Pct Recovery = 93% Analysis Date = 07/26/16 Pct Recovery = 93% Analysis Date = 07/26/16 Pct Recovery = 93% Analysis Date = 07/15/16 Pct Recovery = 92% Analysis Date = 07/15/16 Pct Recovery = 92% Analysis Date = 07/04/16 Pct Recovery = 92% Analysis Date = 07/04/16 Pct Recovery = 92% Analysis Date = 06/24/16 Pct Recovery = 92% Analysis Date = 06/24/16 Pct Recovery = 92% Analysis Date = 06/13/16 Pct Recovery = 92% Analysis Date = 06/13/16 Pct Recovery = 92% Analysis Date = 06/02/16 Pct Recovery = 92% Analysis Date = 06/02/16 Pct Recovery = 92% Analysis Date = 05/23/16 Pct Recovery = 92% Analysis Date = 05/23/16 Pct Recovery = 92% Analysis Date = 05/12/16 Pct Recovery = 92% Analysis Date = 05/12/16 Pct Recovery = 92% Analysis Date = 05/01/16 Pct Recovery = 91% Analysis Date = 05/01/16 Pct Recovery = 91% Analysis Date = 04/21/16 Pct Recovery = 91% Analysis Date = 04/21/16 Pct Recovery = 91% Analysis Date = 04/10/16 Pct Recovery = 91% Analysis Date = 04/10/16 Pct Recovery = 91% Analysis Date = 03/30/16 Pct Recovery = 91% Analysis Date = 03/30/16 Pct Recovery = 91% Analysis Date = 03/19/16 Pct Recovery = 91% Analysis Date = 03/19/16 Pct Recovery = 91% Analysis Date = 03/09/16 Pct Recovery = 91% Analysis Date = 03/09/16 Pct Recovery = 91% Analysis Date = 02/27/16 Pct Recovery = 90% Analysis Date = 02/27/16 Pct Recovery = 90% Analysis Date = 02/16/16 Pct Recovery = 90% Analysis Date = 02/16/16 Pct Recovery = 90% Analysis Date = 02/06/16 Pct Recovery = 90% Analysis Date = 02/06/16 Pct Recovery = 90% Analysis Date = 01/26/16 Pct Recovery = 90% Analysis Date = 01/26/16 Pct Recovery = 90% Analysis Date = 01/15/16 Pct Recovery = 90% Analysis Date = 01/15/16 Pct Recovery = 90% Analysis Date = 01/05/16 Pct Recovery = 90% Analysis Date = 01/05/16 Pct Recovery = 90% Analysis Date = 12/25/15 Pct Recovery = 89% Analysis Date = 12/25/15 Pct Recovery = 89% Analysis Date = 12/14/15 Pct Recovery = 89% Analysis Date = 12/14/15 Pct Recovery = 89% Analysis Date = 12/04/15 Pct Recovery = 89% Analysis Date = 12/04/15 Pct Recovery = 89% Analysis Date = 11/23/15 Pct Recovery = 89% Analysis Date = 11/23/15 Pct Recovery = 89% Analysis Date = 11/12/15 Pct Recovery = 89% Analysis Date = 11/12/15 Pct Recovery = 89% Analysis Date = 11/02/15 Pct Recovery = 88% Analysis Date = 11/02/15 Pct Recovery = 88% Analysis Date = 10/22/15 Pct Recovery = 88% Analysis Date = 10/22/15 Pct Recovery = 88% Analysis Date = 10/11/15 Pct Recovery = 88% Analysis Date = 10/11/15 Pct Recovery = 88% Analysis Date = 10/01/15 Pct Recovery = 88% Analysis Date = 10/01/15 Pct Recovery = 88% Analysis Date = 09/20/15 Pct Recovery = 88% Analysis Date = 09/20/15 Pct Recovery = 88% Analysis Date = 09/09/15 Pct Recovery = 87% Analysis Date = 09/09/15 Pct Recovery = 87% Analysis Date = 08/30/15 Pct Recovery = 87% Analysis Date = 08/30/15 Pct Recovery = 87% Analysis Date = 08/19/15 Pct Recovery = 87% Analysis Date = 08/19/15 Pct Recovery = 87% Analysis Date = 08/08/15 Pct Recovery = 87% Analysis Date = 08/08/15 Pct Recovery = 87% Analysis Date = 07/29/15 Pct Recovery = 87% Analysis Date = 07/29/15 Pct Recovery = 87% Analysis Date = 07/18/15 Pct Recovery = 86% Analysis Date = 07/18/15 Pct Recovery = 86% Analysis Date = 07/07/15 Pct Recovery = 86% Analysis Date = 07/07/15 Pct Recovery = 86% Analysis Date = 06/26/15 Pct Recovery = 86% Analysis Date = 06/26/15 Pct Recovery = 86% Analysis Date = 06/16/15 Pct Recovery = 86% Analysis Date = 06/16/15 Pct Recovery = 86% Analysis Date = 06/05/15 Pct Recovery = 86% Analysis Date = 06/05/15 Pct Recovery = 86% Analysis Date = 05/25/15 Pct Recovery = 85% Analysis Date = 05/25/15 Pct Recovery = 85% Analysis Date = 05/15/15 Pct Recovery = 85% Analysis Date = 05/15/15 Pct Recovery = 85% Analysis Date = 05/04/15 Pct Recovery = 85% Analysis Date = 05/04/15 Pct Recovery = 85% Analysis Date = 04/23/15 Pct Recovery = 85% Analysis Date = 04/23/15 Pct Recovery = 85% Analysis Date = 04/13/15 Pct Recovery = 84% Analysis Date = 04/13/15 Pct Recovery = 84% Analysis Date = 04/02/15 Pct Recovery = 84% Analysis Date = 04/02/15 Pct Recovery = 84% Analysis Date = 03/22/15 Pct Recovery = 84% Analysis Date = 03/22/15 Pct Recovery = 84% Analysis Date = 03/12/15 Pct Recovery = 84% Analysis Date = 03/12/15 Pct Recovery = 84% Analysis Date = 03/01/15 Pct Recovery = 83% Analysis Date = 03/01/15 Pct Recovery = 83% Analysis Date = 02/18/15 Pct Recovery = 83% Analysis Date = 02/18/15 Pct Recovery = 83% Analysis Date = 02/08/15 Pct Recovery = 83% Analysis Date = 02/08/15 Pct Recovery = 83% Analysis Date = 01/28/15 Pct Recovery = 83% Analysis Date = 01/28/15 Pct Recovery = 83% Analysis Date = 01/17/15 Pct Recovery = 82% Analysis Date = 01/17/15 Pct Recovery = 82% Analysis Date = 01/07/15 Pct Recovery = 82% Analysis Date = 01/07/15 Pct Recovery = 82% Analysis Date = 12/27/14 Pct Recovery = 82% Analysis Date = 12/27/14 Pct Recovery = 82% Analysis Date = 12/16/14 Pct Recovery = 81% Analysis Date = 12/16/14 Pct Recovery = 81% Analysis Date = 12/06/14 Pct Recovery = 81% Analysis Date = 12/06/14 Pct Recovery = 81% Analysis Date = 11/25/14 Pct Recovery = 81% Analysis Date = 11/25/14 Pct Recovery = 81% Analysis Date = 11/14/14 Pct Recovery = 81% Analysis Date = 11/14/14 Pct Recovery = 81% Analysis Date = 11/04/14 Pct Recovery = 80% Analysis Date = 11/04/14 Pct Recovery = 80% Analysis Date = 10/24/14 Pct Recovery = 80% Analysis Date = 10/24/14 Pct Recovery = 80% Analysis Date = 10/13/14 Pct Recovery = 80% Analysis Date = 10/13/14 Pct Recovery = 80% Analysis Date = 10/02/14 Pct Recovery = 79% Analysis Date = 10/02/14 Pct Recovery = 79% Analysis Date = 09/22/14 Pct Recovery = 79% Analysis Date = 09/22/14 Pct Recovery = 79% Analysis Date = 09/11/14 Pct Recovery = 79% Analysis Date = 09/11/14 Pct Recovery = 79% Analysis Date = 08/31/14 Pct Recovery = 78% Analysis Date = 08/31/14 Pct Recovery = 78% Analysis Date = 08/21/14 Pct Recovery = 78% Analysis Date = 08/21/14 Pct Recovery = 78% Analysis Date = 08/10/14 Pct Recovery = 78% Analysis Date = 08/10/14 Pct Recovery = 78% Analysis Date = 07/30/14 Pct Recovery = 77% Analysis Date = 07/30/14 Pct Recovery = 77% Analysis Date = 07/20/14 Pct Recovery = 77% Analysis Date = 07/20/14 Pct Recovery = 77% Analysis Date = 07/09/14 Pct Recovery = 77% Analysis Date = 07/09/14 Pct Recovery = 77% Analysis Date = 06/28/14 Pct Recovery = 77% Analysis Date = 06/28/14 Pct Recovery = 77% Analysis Date = 06/18/14 Pct Recovery = 76% Analysis Date = 06/18/14 Pct Recovery = 76% Analysis Date = 06/07/14 Pct Recovery = 76% Analysis Date = 06/07/14 Pct Recovery = 76% Analysis Date = 05/27/14 Pct Recovery = 76% Analysis Date = 05/27/14 Pct Recovery = 76% Analysis Date = 05/17/14 Pct Recovery = 76% Analysis Date = 05/17/14 Pct Recovery = 76% Analysis Date = 05/06/14 Pct Recovery = 76% Analysis Date = 05/06/14 Pct Recovery = 76% Analysis Date = 04/25/14 Pct Recovery = 76% Analysis Date = 04/25/14 Pct Recovery = 76% Analysis Date = 04/15/14 Pct Recovery = 75% Analysis Date = 04/15/14 Pct Recovery = 75% Analysis Date = 04/04/14 Pct Recovery = 75% Analysis Date = 04/04/14 Pct Recovery = 75% Analysis Date = 03/24/14 Pct Recovery = 75% Analysis Date = 03/24/14 Pct Recovery = 75% Analysis Date = 03/14/14 Pct Recovery = 75% Analysis Date = 03/14/14 Pct Recovery = 75% Analysis Date = 03/03/14 Pct Recovery = 75% Analysis Date = 03/03/14 Pct Recovery = 75% Analysis Date = 02/20/14 Pct Recovery = 75% Analysis Date = 02/20/14 Pct Recovery = 75% Analysis Date = 02/10/14 Pct Recovery = 74% Analysis Date = 02/10/14 Pct Recovery = 74% Analysis Date = 01/30/14 Pct Recovery = 74% Analysis Date = 01/30/14 Pct Recovery = 74% Analysis Date = 01/19/14 Pct Recovery = 74% Analysis Date = 01/19/14 Pct Recovery = 74% Analysis Date = 01/08/14 Pct Recovery = 74% Analysis Date = 01/08/14 Pct Recovery = 74% Analysis Date = 12/29/13 Pct Recovery = 74% Analysis Date = 12/29/13 Pct Recovery = 74% Analysis Date = 12/18/13 Pct Recovery = 74% Analysis Date = 12/18/13 Pct Recovery = 74% Analysis Date = 12/07/13 Pct Recovery = 74% Analysis Date = 12/07/13 Pct Recovery = 74% Analysis Date = 11/27/13 Pct Recovery = 74% Analysis Date = 11/27/13 Pct Recovery = 74% Analysis Date = 11/16/13 Pct Recovery = 74% Analysis Date = 11/16/13 Pct Recovery = 74% Analysis Date = 11/05/13 Pct Recovery = 74% Analysis Date = 11/05/13 Pct Recovery = 74% Analysis Date = 10/26/13 Pct Recovery = 74% Analysis Date = 10/26/13 Pct Recovery = 74% Analysis Date = 10/15/13 Pct Recovery = 74% Analysis Date = 10/15/13 Pct Recovery = 74% Analysis Date = 10/04/13 Pct Recovery = 74% Analysis Date = 10/04/13 Pct Recovery = 74% Analysis Date = 09/24/13 Pct Recovery = 74% Analysis Date = 09/24/13 Pct Recovery = 74% Analysis Date = 09/13/13 Pct Recovery = 74% Analysis Date = 09/13/13 Pct Recovery = 74% Analysis Date = 09/02/13 Pct Recovery = 74% Analysis Date = 09/02/13 Pct Recovery = 74% Analysis Date = 08/23/13 Pct Recovery = 74% Analysis Date = 08/23/13 Pct Recovery = 74% Analysis Date = 08/12/13 Pct Recovery = 74% Analysis Date = 08/12/13 Pct Recovery = 74% Analysis Date = 08/01/13 Pct Recovery = 74% Analysis Date = 08/01/13 Pct Recovery = 74% Analysis Date = 07/22/13 Pct Recovery = 74% Analysis Date = 07/22/13 Pct Recovery = 74% Analysis Date = 07/11/13 Pct Recovery = 74% Analysis Date = 07/11/13 Pct Recovery = 74% Analysis Date = 06/30/13 Pct Recovery = 74% Analysis Date = 06/30/13 Pct Recovery = 74% Analysis Date = 06/20/13 Pct Recovery = 74% Analysis Date = 06/20/13 Pct Recovery = 74% Analysis Date = 06/09/13 Pct Recovery = 74% Analysis Date = 06/09/13 Pct Recovery = 74% Analysis Date = 05/29/13 Pct Recovery = 74% Analysis Date = 05/29/13 Pct Recovery = 74% Analysis Date = 05/19/13 Pct Recovery = 74% Analysis Date = 05/19/13 Pct Recovery = 74% Analysis Date = 05/08/13 Pct Recovery = 75% Analysis Date = 05/08/13 Pct Recovery = 75% Analysis Date = 04/27/13 Pct Recovery = 75% Analysis Date = 04/27/13 Pct Recovery = 75% Analysis Date = 04/16/13 Pct Recovery = 75% Analysis Date = 04/16/13 Pct Recovery = 75% Analysis Date = 04/06/13 Pct Recovery = 75% Analysis Date = 04/06/13 Pct Recovery = 75% Analysis Date = 03/26/13 Pct Recovery = 75% Analysis Date = 03/26/13 Pct Recovery = 75% Analysis Date = 03/15/13 Pct Recovery = 75% Analysis Date = 03/15/13 Pct Recovery = 75% Analysis Date = 03/05/13 Pct Recovery = 75% Analysis Date = 03/05/13 Pct Recovery = 75% Analysis Date = 02/22/13 Pct Recovery = 75% Analysis Date = 02/22/13 Pct Recovery = 75% Analysis Date = 02/11/13 Pct Recovery = 76% Analysis Date = 02/11/13 Pct Recovery = 76% Analysis Date = 02/01/13 Pct Recovery = 76% Analysis Date = 02/01/13 Pct Recovery = 76% Analysis Date = 01/21/13 Pct Recovery = 76% Analysis Date = 01/21/13 Pct Recovery = 76% Analysis Date = 01/10/13 Pct Recovery = 76% Analysis Date = 01/10/13 Pct Recovery = 76% Analysis Date = 12/31/12 Pct Recovery = 76% Analysis Date = 12/31/12 Pct Recovery = 76% Analysis Date = 12/20/12 Pct Recovery = 76% Analysis Date = 12/20/12 Pct Recovery = 76% Analysis Date = 12/09/12 Pct Recovery = 77% Analysis Date = 12/09/12 Pct Recovery = 77% Analysis Date = 11/29/12 Pct Recovery = 77% Analysis Date = 11/29/12 Pct Recovery = 77% Analysis Date = 11/18/12 Pct Recovery = 77% Analysis Date = 11/18/12 Pct Recovery = 77% Analysis Date = 11/07/12 Pct Recovery = 77% Analysis Date = 11/07/12 Pct Recovery = 77% Analysis Date = 10/28/12 Pct Recovery = 77% Analysis Date = 10/28/12 Pct Recovery = 77% Analysis Date = 10/17/12 Pct Recovery = 77% Analysis Date = 10/17/12 Pct Recovery = 77% Analysis Date = 10/06/12 Pct Recovery = 77% Analysis Date = 10/06/12 Pct Recovery = 77% Analysis Date = 09/26/12 Pct Recovery = 77% Analysis Date = 09/26/12 Pct Recovery = 77% Analysis Date = 09/15/12 Pct Recovery = 77% Analysis Date = 09/15/12 Pct Recovery = 77% Analysis Date = 09/04/12 Pct Recovery = 77% Analysis Date = 09/04/12 Pct Recovery = 77% Analysis Date = 08/25/12 Pct Recovery = 78% Analysis Date = 08/25/12 Pct Recovery = 78% Analysis Date = 08/14/12 Pct Recovery = 78% Analysis Date = 08/14/12 Pct Recovery = 78% Analysis Date = 08/03/12 Pct Recovery = 78% Analysis Date = 08/03/12 Pct Recovery = 78% Analysis Date = 07/23/12 Pct Recovery = 78% Analysis Date = 07/23/12 Pct Recovery = 78% Analysis Date = 07/13/12 Pct Recovery = 78% Analysis Date = 07/13/12 Pct Recovery = 78% Analysis Date = 07/02/12 Pct Recovery = 78% Analysis Date = 07/02/12 Pct Recovery = 78% Analysis Date = 06/21/12 Pct Recovery = 78% Analysis Date = 06/21/12 Pct Recovery = 78% Analysis Date = 06/11/12 Pct Recovery = 78% Analysis Date = 06/11/12 Pct Recovery = 78% Analysis Date = 05/31/12 Pct Recovery = 78% Analysis Date = 05/31/12 Pct Recovery = 78% Analysis Date = 05/20/12 Pct Recovery = 79% Analysis Date = 05/20/12 Pct Recovery = 79% Analysis Date = 05/10/12 Pct Recovery = 79% Analysis Date = 05/10/12 Pct Recovery = 79% Analysis Date = 04/29/12 Pct Recovery = 79% Analysis Date = 04/29/12 Pct Recovery = 79% Analysis Date = 04/18/12 Pct Recovery = 79% Analysis Date = 04/18/12 Pct Recovery = 79% Analysis Date = 04/08/12 Pct Recovery = 79% Analysis Date = 04/08/12 Pct Recovery = 79% Analysis Date = 03/28/12 Pct Recovery = 79% Analysis Date = 03/28/12 Pct Recovery = 79% Analysis Date = 03/17/12 Pct Recovery = 79% Analysis Date = 03/17/12 Pct Recovery = 79% Analysis Date = 03/07/12 Pct Recovery = 79% Analysis Date = 03/07/12 Pct Recovery = 79% Analysis Date = 02/25/12 Pct Recovery = 79% Analysis Date = 02/25/12 Pct Recovery = 79% Analysis Date = 02/14/12 Pct Recovery = 80% Analysis Date = 02/14/12 Pct Recovery = 80% Analysis Date = 02/04/12 Pct Recovery = 80% Analysis Date = 02/04/12 Pct Recovery = 80% Analysis Date = 01/24/12 Pct Recovery = 80% Analysis Date = 01/24/12 Pct Recovery = 80% Analysis Date = 01/13/12 Pct Recovery = 80% Analysis Date = 01/13/12 Pct Recovery = 80% Analysis Date = 01/03/12 Pct Recovery = 80% Analysis Date = 01/03/12 Pct Recovery = 80% Analysis Date = 12/23/11 Pct Recovery = 80% Analysis Date = 12/23/11 Pct Recovery = 80% Analysis Date = 12/12/11 Pct Recovery = 80% Analysis Date = 12/12/11 Pct Recovery = 80% Analysis Date = 12/02/11 Pct Recovery = 80% Analysis Date = 12/02/11 Pct Recovery = 80% Analysis Date = 11/21/11 Pct Recovery = 80% Analysis Date = 11/21/11 Pct Recovery = 80% Analysis Date = 11/10/11 Pct Recovery = 81% Analysis Date = 11/10/11 Pct Recovery = 81% Analysis Date = 10/30/11 Pct Recovery = 81% Analysis Date = 10/30/11 Pct Recovery = 81% Analysis Date = 10/20/11 Pct Recovery = 81% Analysis Date = 10/20/11 Pct Recovery = 81% Analysis Date = 10/09/11 Pct Recovery = 81% Analysis Date = 10/09/11 Pct Recovery = 81% Analysis Date = 09/28/11 Pct Recovery = 81% Analysis Date = 09/28/11 Pct Recovery = 81% Analysis Date = 09/18/11 Pct Recovery = 81% Analysis Date = 09/18/11 Pct Recovery = 81% Analysis Date = 09/07/11 Pct Recovery = 81% Analysis Date = 09/07/11 Pct Recovery = 81% Analysis Date = 08/27/11 Pct Recovery = 81% Analysis Date = 08/27/11 Pct Recovery = 81% Analysis Date = 08/17/11 Pct Recovery = 81% Analysis Date = 08/17/11 Pct Recovery = 81% Analysis Date = 08/06/11 Pct Recovery = 81% Analysis Date = 08/06/11 Pct Recovery = 81% Analysis Date = 07/26/11 Pct Recovery = 81% Analysis Date = 07/26/11 Pct Recovery = 81% Analysis Date = 07/16/11 Pct Recovery = 82% Analysis Date = 07/16/11 Pct Recovery = 82% Analysis Date = 07/05/11 Pct Recovery = 82% Analysis Date = 07/05/11 Pct Recovery = 82% Analysis Date = 06/24/11 Pct Recovery = 82% Analysis Date = 06/24/11 Pct Recovery = 82% Analysis Date = 06/14/11 Pct Recovery = 82% Analysis Date = 06/14/11 Pct Recovery = 82% Analysis Date = 06/03/11 Pct Recovery = 82% Analysis Date = 06/03/11 Pct Recovery = 82% Analysis Date = 05/23/11 Pct Recovery = 82% Analysis Date = 05/23/11 Pct Recovery = 82% Analysis Date = 05/13/11 Pct Recovery = 82% Analysis Date = 05/13/11 Pct Recovery = 82% Analysis Date = 05/02/11 Pct Recovery = 82% Analysis Date = 05/02/11 Pct Recovery = 82% Analysis Date = 04/21/11 Pct Recovery = 82% Analysis Date = 04/21/11 Pct Recovery = 82% Analysis Date = 04/11/11 Pct Recovery = 82% Analysis Date = 04/11/11 Pct Recovery = 82% Analysis Date = 03/31/11 Pct Recovery = 82% Analysis Date = 03/31/11 Pct Recovery = 82% Analysis Date = 03/20/11 Pct Recovery = 82% Analysis Date = 03/20/11 Pct Recovery = 82% Analysis Date = 03/10/11 Pct Recovery = 83% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
ESTRIOL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 72 82% 16% 81% 15%
Total 72 82% 16% 81% 15%

Sample Statistics
ESTRIOL

Characteristic N % % Basis
Plotted 72 92% Spiked
Estimated Values 1 1% Spiked
Deleted Values 2 2% Spiked + Not Spiked
Spiked, Censored 1 1% Spiked
Spiked 80 .  
False Negatives 5 6% 5 out of 78
Not Spiked 51 .  
False Positives 0 0% 0 out of 51

BQS OBSP Determination:
ESTRONE
METHOD: 4434 , TESTIDCODE: 64541GM005
Open Data Set

Analysis Date = 08/31/16 SpikeMix = Spex Organics TS160420010: 50 µl & ChemService 5016200: 50 µl Pct Recovery = 48% Analysis Date = 08/19/16 SpikeMix = Supelco LC20140V: 50 µl & Spex Organics TS160420010: 50 µl Pct Recovery = 66% Analysis Date = 08/11/16 SpikeMix = ChemService 5016100: 50 µl & Spex Organics TS160420010: 50 µl Pct Recovery = 53% Analysis Date = 12/03/12 SpikeMix = ERA 0511-12-02: 50 µl & Abs 051512: 50 µl Pct Recovery = 67% Analysis Date = 11/07/12 SpikeMix = ERA 0507-12-04.1: 50 µl & ERA 0511-12-02: 50 µl Pct Recovery = 85% Analysis Date = 04/22/13 SpikeMix = ERA 0507-12-04.1: 50 µl & Restek A089631: 50 µl Pct Recovery = 65% Analysis Date = 04/03/13 SpikeMix = Spex Organics T1120525010: 50 µl & Restek A089631: 50 µl Pct Recovery = 73% Analysis Date = 02/22/13 SpikeMix = Restek A089631: 50 µl & Supelco LB92781: 50 µl Pct Recovery = 68% Analysis Date = 12/18/12 SpikeMix = ERA 0507-12-04.1: 50 µl & Restek A089631: 50 µl Pct Recovery = 76% Analysis Date = 01/27/12 SpikeMix = Supelco LB77167: 100 µl Pct Recovery = 75% Analysis Date = 10/13/11 SpikeMix = Supelco LB77167: 100 µl Pct Recovery = 74% Analysis Date = 03/27/12 SpikeMix = Crescent 162776: 100 µl Pct Recovery = 94% Analysis Date = 06/07/11 SpikeMix = Supelco LB77167: 100 µl Pct Recovery = 76% Analysis Date = 03/10/11 SpikeMix = Crescent 162776: 100 µl Pct Recovery = 71% Analysis Date = 06/23/11 SpikeMix = Crescent 162776: 100 µl Pct Recovery = 81% Analysis Date = 04/14/14 SpikeMix = ERA 0415-13-01.1A: 50 µl & Abs 071513: 50 µl Pct Recovery = 108% Analysis Date = 03/14/14 SpikeMix = Supelco LB99393: 50 µl & Abs 060413: 50 µl & Abs 071513: 50 µl Pct Recovery = 55% Analysis Date = 03/05/14 SpikeMix = ERA 0415-13-01.1A: 50 µl & Abs 060413: 50 µl & Abs 071513: 50 µl Pct Recovery = 63% Analysis Date = 03/05/14 SpikeMix = Spex Organics T1130423008: 50 µl & Abs 071513: 50 µl Pct Recovery = 70% Analysis Date = 03/14/14 SpikeMix = ERA 0415-13-01.2A: 50 µl & Spex Organics T1130423008: 50 µl Pct Recovery = 49% Analysis Date = 08/09/13 SpikeMix = ERA 0415-13-01.2A: 50 µl & Spex Organics T1130423008: 50 µl Pct Recovery = 69% Analysis Date = 04/10/13 SpikeMix = ERA 0511-12-02: 25 µl & Supelco LB92781: 25 µl Pct Recovery = 86% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120525010: 25 µl & ERA 0511-12-02: 25 µl Pct Recovery = 64% Analysis Date = 08/31/12 SpikeMix = ERA 0511-12-02: 25 µl & Abs 051512: 25 µl Pct Recovery = 95% Analysis Date = 12/18/12 SpikeMix = Restek A089631: 25 µl & Supelco LB92781: 25 µl Pct Recovery = 76% Analysis Date = 04/01/15 SpikeMix = ERA 0227-14-07.2: 60 µl & ChemService 2561700: 60 µl Pct Recovery = 80% Analysis Date = 08/22/14 SpikeMix = ERA 0227-14-07.2: 60 µl & Abs 042114: 60 µl Pct Recovery = 108% Analysis Date = 04/01/15 SpikeMix = Spex Organics E1140505004: 60 µl & Supelco LC06946: 60 µl Pct Recovery = 42% Analysis Date = 12/09/14 SpikeMix = Abs 031014: 60 µl & Supelco LC06946: 60 µl Pct Recovery = 79% Analysis Date = 09/23/14 SpikeMix = Supelco LC06946: 60 µl & ChemService 2561700: 60 µl Pct Recovery = 77% Analysis Date = 07/27/12 SpikeMix = Supelco LB77167: 25 µl Pct Recovery = 67% Analysis Date = 04/17/12 SpikeMix = Supelco LB77167: 25 µl Pct Recovery = 67% Analysis Date = 04/04/12 SpikeMix = Supelco LB77167: 25 µl Pct Recovery = 97% Analysis Date = 09/29/11 SpikeMix = Supelco LB77167: 25 µl Pct Recovery = 73% Analysis Date = 04/06/12 SpikeMix = Crescent 162776: 25 µl Pct Recovery = 64% Analysis Date = 11/17/11 SpikeMix = Crescent 162776: 25 µl Pct Recovery = 79% Analysis Date = 10/12/11 SpikeMix = Crescent 162776: 25 µl Pct Recovery = 83% Analysis Date = 07/25/11 SpikeMix = Crescent 162776: 25 µl Pct Recovery = 67% Analysis Date = 05/19/11 SpikeMix = Supelco LB77167: 25 µl Pct Recovery = 80% Analysis Date = 03/31/11 SpikeMix = Supelco LB77167: 25 µl Pct Recovery = 82% Analysis Date = 05/09/11 SpikeMix = Crescent 162776: 25 µl Pct Recovery = 74% Analysis Date = 03/03/14 SpikeMix = Abs 050813: 20 µl & Abs 071513: 20 µl Pct Recovery = 57% Analysis Date = 02/19/14 SpikeMix = Abs 050813: 20 µl & Abs 071513: 20 µl Pct Recovery = 51% Analysis Date = 04/14/14 SpikeMix = ERA 0415-13-01.1A: 20 µl & ERA 0415-13-01.2A: 20 µl & Abs 060413: 20 µl Pct Recovery = 90% Analysis Date = 01/23/14 SpikeMix = Supelco LB99393: 20 µl & ERA 0415-13-01.2A: 20 µl & Abs 060413: 20 µl Pct Recovery = 52% Analysis Date = 11/18/13 SpikeMix = ERA 0415-13-01.2A: 20 µl & Abs 050813: 20 µl Pct Recovery = 62% Analysis Date = 09/16/13 SpikeMix = ERA 0415-13-01.1A: 20 µl & ERA 0415-13-01.2A: 20 µl & Abs 060413: 20 µl Pct Recovery = 68% Analysis Date = 07/19/13 SpikeMix = Supelco LB99393: 20 µl & ERA 0415-13-01.2A: 20 µl Pct Recovery = 64% Analysis Date = 01/05/16 SpikeMix = Supelco LC13547: 60 µl & ChemService 4073900: 60 µl Pct Recovery = 76% Analysis Date = 02/01/17 SpikeMix = Supelco LC20140V: 30 µl & Abs 052616: 30 µl Pct Recovery = 69% Analysis Date = 01/13/17 SpikeMix = Abs 052616: 30 µl & ChemService 5016200: 30 µl Pct Recovery = 79% Analysis Date = 12/29/16 SpikeMix = ChemService 5016100: 30 µl & Abs 052616: 30 µl Pct Recovery = 69% Analysis Date = 12/05/16 SpikeMix = Abs 052616: 30 µl & Abs 061416H: 30 µl Pct Recovery = 123% Analysis Date = 06/24/16 SpikeMix = ERA 0601-15-04: 50 µl & ChemService 4073900: 50 µl Pct Recovery = 94% Analysis Date = 03/07/16 SpikeMix = Abs 041515: 50 µl & ERA 0601-15-04: 50 µl Pct Recovery = 59% Analysis Date = 09/14/15 SpikeMix = ERA 0601-15-04: 50 µl & ChemService 4073900: 50 µl Pct Recovery = 112% Analysis Date = 08/10/15 SpikeMix = ERA 0601-15-04: 50 µl & Crescent 04EE007: 50 µl Pct Recovery = 100% Analysis Date = 09/16/16 SpikeMix = Spex Organics EN160621015: 30 µl & ChemService 5016200: 30 µl Pct Recovery = 65% Analysis Date = 11/05/14 SpikeMix = ERA 0227-14-07.2: 30 µl & Abs 042114: 30 µl Pct Recovery = 76% Analysis Date = 09/04/14 SpikeMix = ERA 0227-14-07.2: 30 µl & Spex Organics E1140505004: 30 µl Pct Recovery = 81% Analysis Date = 07/28/14 SpikeMix = ERA 0227-14-07.2: 30 µl & ChemService 2561700: 30 µl Pct Recovery = 94% Analysis Date = 07/14/14 SpikeMix = ERA 0227-14-07.2: 30 µl & Abs 031014: 30 µl Pct Recovery = 78% Analysis Date = 01/21/15 SpikeMix = Supelco LC06946: 30 µl & ChemService 2561700: 30 µl Pct Recovery = 68% Analysis Date = 12/23/14 SpikeMix = Spex Organics E1140505004: 30 µl & Supelco LC06946: 30 µl Pct Recovery = 86% Analysis Date = 12/16/14 SpikeMix = Supelco LC06946: 30 µl & Abs 042114: 30 µl Pct Recovery = 75% Analysis Date = 01/08/16 SpikeMix = ERA 0601-15-04: 30 µl & Crescent 04EE007: 30 µl Pct Recovery = 69% Analysis Date = 02/01/17 Pct Recovery = 74% Analysis Date = 01/21/17 Pct Recovery = 74% Analysis Date = 01/21/17 Pct Recovery = 74% Analysis Date = 01/10/17 Pct Recovery = 74% Analysis Date = 01/10/17 Pct Recovery = 74% Analysis Date = 12/30/16 Pct Recovery = 74% Analysis Date = 12/30/16 Pct Recovery = 74% Analysis Date = 12/19/16 Pct Recovery = 74% Analysis Date = 12/19/16 Pct Recovery = 74% Analysis Date = 12/09/16 Pct Recovery = 74% Analysis Date = 12/09/16 Pct Recovery = 74% Analysis Date = 11/28/16 Pct Recovery = 74% Analysis Date = 11/28/16 Pct Recovery = 74% Analysis Date = 11/17/16 Pct Recovery = 75% Analysis Date = 11/17/16 Pct Recovery = 75% Analysis Date = 11/06/16 Pct Recovery = 75% Analysis Date = 11/06/16 Pct Recovery = 75% Analysis Date = 10/27/16 Pct Recovery = 75% Analysis Date = 10/27/16 Pct Recovery = 75% Analysis Date = 10/16/16 Pct Recovery = 75% Analysis Date = 10/16/16 Pct Recovery = 75% Analysis Date = 10/05/16 Pct Recovery = 75% Analysis Date = 10/05/16 Pct Recovery = 75% Analysis Date = 09/24/16 Pct Recovery = 75% Analysis Date = 09/24/16 Pct Recovery = 75% Analysis Date = 09/13/16 Pct Recovery = 75% Analysis Date = 09/13/16 Pct Recovery = 75% Analysis Date = 09/03/16 Pct Recovery = 75% Analysis Date = 09/03/16 Pct Recovery = 75% Analysis Date = 08/23/16 Pct Recovery = 75% Analysis Date = 08/23/16 Pct Recovery = 75% Analysis Date = 08/12/16 Pct Recovery = 75% Analysis Date = 08/12/16 Pct Recovery = 75% Analysis Date = 08/01/16 Pct Recovery = 75% Analysis Date = 08/01/16 Pct Recovery = 75% Analysis Date = 07/22/16 Pct Recovery = 75% Analysis Date = 07/22/16 Pct Recovery = 75% Analysis Date = 07/11/16 Pct Recovery = 75% Analysis Date = 07/11/16 Pct Recovery = 75% Analysis Date = 06/30/16 Pct Recovery = 75% Analysis Date = 06/30/16 Pct Recovery = 75% Analysis Date = 06/19/16 Pct Recovery = 75% Analysis Date = 06/19/16 Pct Recovery = 75% Analysis Date = 06/08/16 Pct Recovery = 75% Analysis Date = 06/08/16 Pct Recovery = 75% Analysis Date = 05/29/16 Pct Recovery = 75% Analysis Date = 05/29/16 Pct Recovery = 75% Analysis Date = 05/18/16 Pct Recovery = 75% Analysis Date = 05/18/16 Pct Recovery = 75% Analysis Date = 05/07/16 Pct Recovery = 75% Analysis Date = 05/07/16 Pct Recovery = 75% Analysis Date = 04/26/16 Pct Recovery = 75% Analysis Date = 04/26/16 Pct Recovery = 75% Analysis Date = 04/16/16 Pct Recovery = 76% Analysis Date = 04/16/16 Pct Recovery = 76% Analysis Date = 04/05/16 Pct Recovery = 76% Analysis Date = 04/05/16 Pct Recovery = 76% Analysis Date = 03/25/16 Pct Recovery = 76% Analysis Date = 03/25/16 Pct Recovery = 76% Analysis Date = 03/14/16 Pct Recovery = 76% Analysis Date = 03/14/16 Pct Recovery = 76% Analysis Date = 03/03/16 Pct Recovery = 76% Analysis Date = 03/03/16 Pct Recovery = 76% Analysis Date = 02/22/16 Pct Recovery = 76% Analysis Date = 02/22/16 Pct Recovery = 76% Analysis Date = 02/11/16 Pct Recovery = 76% Analysis Date = 02/11/16 Pct Recovery = 76% Analysis Date = 01/31/16 Pct Recovery = 76% Analysis Date = 01/31/16 Pct Recovery = 76% Analysis Date = 01/20/16 Pct Recovery = 76% Analysis Date = 01/20/16 Pct Recovery = 76% Analysis Date = 01/10/16 Pct Recovery = 76% Analysis Date = 01/10/16 Pct Recovery = 76% Analysis Date = 12/30/15 Pct Recovery = 76% Analysis Date = 12/30/15 Pct Recovery = 76% Analysis Date = 12/19/15 Pct Recovery = 76% Analysis Date = 12/19/15 Pct Recovery = 76% Analysis Date = 12/08/15 Pct Recovery = 76% Analysis Date = 12/08/15 Pct Recovery = 76% Analysis Date = 11/28/15 Pct Recovery = 76% Analysis Date = 11/28/15 Pct Recovery = 76% Analysis Date = 11/17/15 Pct Recovery = 76% Analysis Date = 11/17/15 Pct Recovery = 76% Analysis Date = 11/06/15 Pct Recovery = 76% Analysis Date = 11/06/15 Pct Recovery = 76% Analysis Date = 10/26/15 Pct Recovery = 76% Analysis Date = 10/26/15 Pct Recovery = 76% Analysis Date = 10/15/15 Pct Recovery = 76% Analysis Date = 10/15/15 Pct Recovery = 76% Analysis Date = 10/05/15 Pct Recovery = 76% Analysis Date = 10/05/15 Pct Recovery = 76% Analysis Date = 09/24/15 Pct Recovery = 76% Analysis Date = 09/24/15 Pct Recovery = 76% Analysis Date = 09/13/15 Pct Recovery = 76% Analysis Date = 09/13/15 Pct Recovery = 76% Analysis Date = 09/02/15 Pct Recovery = 76% Analysis Date = 09/02/15 Pct Recovery = 76% Analysis Date = 08/23/15 Pct Recovery = 76% Analysis Date = 08/23/15 Pct Recovery = 76% Analysis Date = 08/12/15 Pct Recovery = 76% Analysis Date = 08/12/15 Pct Recovery = 76% Analysis Date = 08/01/15 Pct Recovery = 76% Analysis Date = 08/01/15 Pct Recovery = 76% Analysis Date = 07/21/15 Pct Recovery = 77% Analysis Date = 07/21/15 Pct Recovery = 77% Analysis Date = 07/10/15 Pct Recovery = 77% Analysis Date = 07/10/15 Pct Recovery = 77% Analysis Date = 06/30/15 Pct Recovery = 77% Analysis Date = 06/30/15 Pct Recovery = 77% Analysis Date = 06/19/15 Pct Recovery = 77% Analysis Date = 06/19/15 Pct Recovery = 77% Analysis Date = 06/08/15 Pct Recovery = 77% Analysis Date = 06/08/15 Pct Recovery = 77% Analysis Date = 05/28/15 Pct Recovery = 77% Analysis Date = 05/28/15 Pct Recovery = 77% Analysis Date = 05/18/15 Pct Recovery = 77% Analysis Date = 05/18/15 Pct Recovery = 77% Analysis Date = 05/07/15 Pct Recovery = 77% Analysis Date = 05/07/15 Pct Recovery = 77% Analysis Date = 04/26/15 Pct Recovery = 77% Analysis Date = 04/26/15 Pct Recovery = 77% Analysis Date = 04/15/15 Pct Recovery = 77% Analysis Date = 04/15/15 Pct Recovery = 77% Analysis Date = 04/04/15 Pct Recovery = 77% Analysis Date = 04/04/15 Pct Recovery = 77% Analysis Date = 03/25/15 Pct Recovery = 77% Analysis Date = 03/25/15 Pct Recovery = 77% Analysis Date = 03/14/15 Pct Recovery = 77% Analysis Date = 03/14/15 Pct Recovery = 77% Analysis Date = 03/03/15 Pct Recovery = 77% Analysis Date = 03/03/15 Pct Recovery = 77% Analysis Date = 02/20/15 Pct Recovery = 77% Analysis Date = 02/20/15 Pct Recovery = 77% Analysis Date = 02/10/15 Pct Recovery = 77% Analysis Date = 02/10/15 Pct Recovery = 77% Analysis Date = 01/30/15 Pct Recovery = 78% Analysis Date = 01/30/15 Pct Recovery = 78% Analysis Date = 01/19/15 Pct Recovery = 78% Analysis Date = 01/19/15 Pct Recovery = 78% Analysis Date = 01/08/15 Pct Recovery = 77% Analysis Date = 01/08/15 Pct Recovery = 77% Analysis Date = 12/28/14 Pct Recovery = 77% Analysis Date = 12/28/14 Pct Recovery = 77% Analysis Date = 12/18/14 Pct Recovery = 77% Analysis Date = 12/18/14 Pct Recovery = 77% Analysis Date = 12/07/14 Pct Recovery = 77% Analysis Date = 12/07/14 Pct Recovery = 77% Analysis Date = 11/26/14 Pct Recovery = 77% Analysis Date = 11/26/14 Pct Recovery = 77% Analysis Date = 11/15/14 Pct Recovery = 77% Analysis Date = 11/15/14 Pct Recovery = 77% Analysis Date = 11/05/14 Pct Recovery = 77% Analysis Date = 11/05/14 Pct Recovery = 77% Analysis Date = 10/25/14 Pct Recovery = 77% Analysis Date = 10/25/14 Pct Recovery = 77% Analysis Date = 10/14/14 Pct Recovery = 77% Analysis Date = 10/14/14 Pct Recovery = 77% Analysis Date = 10/03/14 Pct Recovery = 76% Analysis Date = 10/03/14 Pct Recovery = 76% Analysis Date = 09/23/14 Pct Recovery = 76% Analysis Date = 09/23/14 Pct Recovery = 76% Analysis Date = 09/12/14 Pct Recovery = 76% Analysis Date = 09/12/14 Pct Recovery = 76% Analysis Date = 09/01/14 Pct Recovery = 76% Analysis Date = 09/01/14 Pct Recovery = 76% Analysis Date = 08/21/14 Pct Recovery = 75% Analysis Date = 08/21/14 Pct Recovery = 75% Analysis Date = 08/10/14 Pct Recovery = 75% Analysis Date = 08/10/14 Pct Recovery = 75% Analysis Date = 07/31/14 Pct Recovery = 75% Analysis Date = 07/31/14 Pct Recovery = 75% Analysis Date = 07/20/14 Pct Recovery = 75% Analysis Date = 07/20/14 Pct Recovery = 75% Analysis Date = 07/09/14 Pct Recovery = 75% Analysis Date = 07/09/14 Pct Recovery = 75% Analysis Date = 06/28/14 Pct Recovery = 74% Analysis Date = 06/28/14 Pct Recovery = 74% Analysis Date = 06/18/14 Pct Recovery = 74% Analysis Date = 06/18/14 Pct Recovery = 74% Analysis Date = 06/07/14 Pct Recovery = 74% Analysis Date = 06/07/14 Pct Recovery = 74% Analysis Date = 05/27/14 Pct Recovery = 74% Analysis Date = 05/27/14 Pct Recovery = 74% Analysis Date = 05/16/14 Pct Recovery = 74% Analysis Date = 05/16/14 Pct Recovery = 74% Analysis Date = 05/05/14 Pct Recovery = 74% Analysis Date = 05/05/14 Pct Recovery = 74% Analysis Date = 04/25/14 Pct Recovery = 73% Analysis Date = 04/25/14 Pct Recovery = 73% Analysis Date = 04/14/14 Pct Recovery = 73% Analysis Date = 04/14/14 Pct Recovery = 73% Analysis Date = 04/03/14 Pct Recovery = 73% Analysis Date = 04/03/14 Pct Recovery = 73% Analysis Date = 03/23/14 Pct Recovery = 73% Analysis Date = 03/23/14 Pct Recovery = 73% Analysis Date = 03/13/14 Pct Recovery = 73% Analysis Date = 03/13/14 Pct Recovery = 73% Analysis Date = 03/02/14 Pct Recovery = 73% Analysis Date = 03/02/14 Pct Recovery = 73% Analysis Date = 02/19/14 Pct Recovery = 73% Analysis Date = 02/19/14 Pct Recovery = 73% Analysis Date = 02/08/14 Pct Recovery = 72% Analysis Date = 02/08/14 Pct Recovery = 72% Analysis Date = 01/28/14 Pct Recovery = 72% Analysis Date = 01/28/14 Pct Recovery = 72% Analysis Date = 01/18/14 Pct Recovery = 72% Analysis Date = 01/18/14 Pct Recovery = 72% Analysis Date = 01/07/14 Pct Recovery = 72% Analysis Date = 01/07/14 Pct Recovery = 72% Analysis Date = 12/27/13 Pct Recovery = 72% Analysis Date = 12/27/13 Pct Recovery = 72% Analysis Date = 12/16/13 Pct Recovery = 72% Analysis Date = 12/16/13 Pct Recovery = 72% Analysis Date = 12/06/13 Pct Recovery = 72% Analysis Date = 12/06/13 Pct Recovery = 72% Analysis Date = 11/25/13 Pct Recovery = 72% Analysis Date = 11/25/13 Pct Recovery = 72% Analysis Date = 11/14/13 Pct Recovery = 72% Analysis Date = 11/14/13 Pct Recovery = 72% Analysis Date = 11/03/13 Pct Recovery = 72% Analysis Date = 11/03/13 Pct Recovery = 72% Analysis Date = 10/23/13 Pct Recovery = 71% Analysis Date = 10/23/13 Pct Recovery = 71% Analysis Date = 10/13/13 Pct Recovery = 71% Analysis Date = 10/13/13 Pct Recovery = 71% Analysis Date = 10/02/13 Pct Recovery = 71% Analysis Date = 10/02/13 Pct Recovery = 71% Analysis Date = 09/21/13 Pct Recovery = 71% Analysis Date = 09/21/13 Pct Recovery = 71% Analysis Date = 09/10/13 Pct Recovery = 71% Analysis Date = 09/10/13 Pct Recovery = 71% Analysis Date = 08/31/13 Pct Recovery = 71% Analysis Date = 08/31/13 Pct Recovery = 71% Analysis Date = 08/20/13 Pct Recovery = 71% Analysis Date = 08/20/13 Pct Recovery = 71% Analysis Date = 08/09/13 Pct Recovery = 71% Analysis Date = 08/09/13 Pct Recovery = 71% Analysis Date = 07/29/13 Pct Recovery = 71% Analysis Date = 07/29/13 Pct Recovery = 71% Analysis Date = 07/19/13 Pct Recovery = 71% Analysis Date = 07/19/13 Pct Recovery = 71% Analysis Date = 07/08/13 Pct Recovery = 71% Analysis Date = 07/08/13 Pct Recovery = 71% Analysis Date = 06/27/13 Pct Recovery = 71% Analysis Date = 06/27/13 Pct Recovery = 71% Analysis Date = 06/16/13 Pct Recovery = 71% Analysis Date = 06/16/13 Pct Recovery = 71% Analysis Date = 06/05/13 Pct Recovery = 71% Analysis Date = 06/05/13 Pct Recovery = 71% Analysis Date = 05/26/13 Pct Recovery = 71% Analysis Date = 05/26/13 Pct Recovery = 71% Analysis Date = 05/15/13 Pct Recovery = 71% Analysis Date = 05/15/13 Pct Recovery = 71% Analysis Date = 05/04/13 Pct Recovery = 72% Analysis Date = 05/04/13 Pct Recovery = 72% Analysis Date = 04/23/13 Pct Recovery = 72% Analysis Date = 04/23/13 Pct Recovery = 72% Analysis Date = 04/13/13 Pct Recovery = 72% Analysis Date = 04/13/13 Pct Recovery = 72% Analysis Date = 04/02/13 Pct Recovery = 72% Analysis Date = 04/02/13 Pct Recovery = 72% Analysis Date = 03/22/13 Pct Recovery = 72% Analysis Date = 03/22/13 Pct Recovery = 72% Analysis Date = 03/11/13 Pct Recovery = 72% Analysis Date = 03/11/13 Pct Recovery = 72% Analysis Date = 02/28/13 Pct Recovery = 72% Analysis Date = 02/28/13 Pct Recovery = 72% Analysis Date = 02/18/13 Pct Recovery = 73% Analysis Date = 02/18/13 Pct Recovery = 73% Analysis Date = 02/07/13 Pct Recovery = 73% Analysis Date = 02/07/13 Pct Recovery = 73% Analysis Date = 01/27/13 Pct Recovery = 73% Analysis Date = 01/27/13 Pct Recovery = 73% Analysis Date = 01/16/13 Pct Recovery = 73% Analysis Date = 01/16/13 Pct Recovery = 73% Analysis Date = 01/06/13 Pct Recovery = 73% Analysis Date = 01/06/13 Pct Recovery = 73% Analysis Date = 12/26/12 Pct Recovery = 73% Analysis Date = 12/26/12 Pct Recovery = 73% Analysis Date = 12/15/12 Pct Recovery = 74% Analysis Date = 12/15/12 Pct Recovery = 74% Analysis Date = 12/04/12 Pct Recovery = 74% Analysis Date = 12/04/12 Pct Recovery = 74% Analysis Date = 11/23/12 Pct Recovery = 74% Analysis Date = 11/23/12 Pct Recovery = 74% Analysis Date = 11/13/12 Pct Recovery = 74% Analysis Date = 11/13/12 Pct Recovery = 74% Analysis Date = 11/02/12 Pct Recovery = 74% Analysis Date = 11/02/12 Pct Recovery = 74% Analysis Date = 10/22/12 Pct Recovery = 74% Analysis Date = 10/22/12 Pct Recovery = 74% Analysis Date = 10/11/12 Pct Recovery = 74% Analysis Date = 10/11/12 Pct Recovery = 74% Analysis Date = 10/01/12 Pct Recovery = 75% Analysis Date = 10/01/12 Pct Recovery = 75% Analysis Date = 09/20/12 Pct Recovery = 75% Analysis Date = 09/20/12 Pct Recovery = 75% Analysis Date = 09/09/12 Pct Recovery = 75% Analysis Date = 09/09/12 Pct Recovery = 75% Analysis Date = 08/29/12 Pct Recovery = 75% Analysis Date = 08/29/12 Pct Recovery = 75% Analysis Date = 08/18/12 Pct Recovery = 75% Analysis Date = 08/18/12 Pct Recovery = 75% Analysis Date = 08/08/12 Pct Recovery = 75% Analysis Date = 08/08/12 Pct Recovery = 75% Analysis Date = 07/28/12 Pct Recovery = 76% Analysis Date = 07/28/12 Pct Recovery = 76% Analysis Date = 07/17/12 Pct Recovery = 76% Analysis Date = 07/17/12 Pct Recovery = 76% Analysis Date = 07/06/12 Pct Recovery = 76% Analysis Date = 07/06/12 Pct Recovery = 76% Analysis Date = 06/26/12 Pct Recovery = 76% Analysis Date = 06/26/12 Pct Recovery = 76% Analysis Date = 06/15/12 Pct Recovery = 76% Analysis Date = 06/15/12 Pct Recovery = 76% Analysis Date = 06/04/12 Pct Recovery = 76% Analysis Date = 06/04/12 Pct Recovery = 76% Analysis Date = 05/24/12 Pct Recovery = 76% Analysis Date = 05/24/12 Pct Recovery = 76% Analysis Date = 05/14/12 Pct Recovery = 76% Analysis Date = 05/14/12 Pct Recovery = 76% Analysis Date = 05/03/12 Pct Recovery = 76% Analysis Date = 05/03/12 Pct Recovery = 76% Analysis Date = 04/22/12 Pct Recovery = 76% Analysis Date = 04/22/12 Pct Recovery = 76% Analysis Date = 04/11/12 Pct Recovery = 76% Analysis Date = 04/11/12 Pct Recovery = 76% Analysis Date = 03/31/12 Pct Recovery = 76% Analysis Date = 03/31/12 Pct Recovery = 76% Analysis Date = 03/21/12 Pct Recovery = 76% Analysis Date = 03/21/12 Pct Recovery = 76% Analysis Date = 03/10/12 Pct Recovery = 76% Analysis Date = 03/10/12 Pct Recovery = 76% Analysis Date = 02/28/12 Pct Recovery = 76% Analysis Date = 02/28/12 Pct Recovery = 76% Analysis Date = 02/17/12 Pct Recovery = 76% Analysis Date = 02/17/12 Pct Recovery = 76% Analysis Date = 02/07/12 Pct Recovery = 76% Analysis Date = 02/07/12 Pct Recovery = 76% Analysis Date = 01/27/12 Pct Recovery = 77% Analysis Date = 01/27/12 Pct Recovery = 77% Analysis Date = 01/16/12 Pct Recovery = 77% Analysis Date = 01/16/12 Pct Recovery = 77% Analysis Date = 01/05/12 Pct Recovery = 77% Analysis Date = 01/05/12 Pct Recovery = 77% Analysis Date = 12/25/11 Pct Recovery = 77% Analysis Date = 12/25/11 Pct Recovery = 77% Analysis Date = 12/15/11 Pct Recovery = 77% Analysis Date = 12/15/11 Pct Recovery = 77% Analysis Date = 12/04/11 Pct Recovery = 77% Analysis Date = 12/04/11 Pct Recovery = 77% Analysis Date = 11/23/11 Pct Recovery = 77% Analysis Date = 11/23/11 Pct Recovery = 77% Analysis Date = 11/12/11 Pct Recovery = 77% Analysis Date = 11/12/11 Pct Recovery = 77% Analysis Date = 11/02/11 Pct Recovery = 77% Analysis Date = 11/02/11 Pct Recovery = 77% Analysis Date = 10/22/11 Pct Recovery = 77% Analysis Date = 10/22/11 Pct Recovery = 77% Analysis Date = 10/11/11 Pct Recovery = 77% Analysis Date = 10/11/11 Pct Recovery = 77% Analysis Date = 09/30/11 Pct Recovery = 77% Analysis Date = 09/30/11 Pct Recovery = 77% Analysis Date = 09/19/11 Pct Recovery = 77% Analysis Date = 09/19/11 Pct Recovery = 77% Analysis Date = 09/09/11 Pct Recovery = 77% Analysis Date = 09/09/11 Pct Recovery = 77% Analysis Date = 08/29/11 Pct Recovery = 77% Analysis Date = 08/29/11 Pct Recovery = 77% Analysis Date = 08/18/11 Pct Recovery = 77% Analysis Date = 08/18/11 Pct Recovery = 77% Analysis Date = 08/07/11 Pct Recovery = 77% Analysis Date = 08/07/11 Pct Recovery = 77% Analysis Date = 07/28/11 Pct Recovery = 77% Analysis Date = 07/28/11 Pct Recovery = 77% Analysis Date = 07/17/11 Pct Recovery = 77% Analysis Date = 07/17/11 Pct Recovery = 77% Analysis Date = 07/06/11 Pct Recovery = 77% Analysis Date = 07/06/11 Pct Recovery = 77% Analysis Date = 06/25/11 Pct Recovery = 77% Analysis Date = 06/25/11 Pct Recovery = 77% Analysis Date = 06/14/11 Pct Recovery = 77% Analysis Date = 06/14/11 Pct Recovery = 77% Analysis Date = 06/04/11 Pct Recovery = 78% Analysis Date = 06/04/11 Pct Recovery = 78% Analysis Date = 05/24/11 Pct Recovery = 78% Analysis Date = 05/24/11 Pct Recovery = 78% Analysis Date = 05/13/11 Pct Recovery = 78% Analysis Date = 05/13/11 Pct Recovery = 78% Analysis Date = 05/02/11 Pct Recovery = 78% Analysis Date = 05/02/11 Pct Recovery = 78% Analysis Date = 04/22/11 Pct Recovery = 78% Analysis Date = 04/22/11 Pct Recovery = 78% Analysis Date = 04/11/11 Pct Recovery = 78% Analysis Date = 04/11/11 Pct Recovery = 78% Analysis Date = 03/31/11 Pct Recovery = 78% Analysis Date = 03/31/11 Pct Recovery = 78% Analysis Date = 03/20/11 Pct Recovery = 78% Analysis Date = 03/20/11 Pct Recovery = 78% Analysis Date = 03/10/11 Pct Recovery = 78% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
ESTRONE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 66 75% 16% 74% 11%
Total 66 75% 16% 74% 11%

Sample Statistics
ESTRONE

Characteristic N % % Basis
Plotted 66 80% Spiked
Estimated Values 5 6% Spiked
Deleted Values 3 2% Spiked + Not Spiked
Spiked, Censored 5 6% Spiked
Spiked 83 .  
False Negatives 11 13% 11 out of 82
Not Spiked 48 .  
False Positives 0 0% 0 out of 46

BQS OBSP Determination:
MESTRANOL
METHOD: 4434 , TESTIDCODE: 64542GM005
Open Data Set

Analysis Date = 08/31/16 SpikeMix = Spex Organics TS160420010: 50 µl & ChemService 5016200: 50 µl Pct Recovery = 51% Analysis Date = 08/19/16 SpikeMix = Supelco LC20140V: 50 µl & Spex Organics TS160420010: 50 µl Pct Recovery = 55% Analysis Date = 08/11/16 SpikeMix = ChemService 5016100: 50 µl & Spex Organics TS160420010: 50 µl Pct Recovery = 32% Analysis Date = 12/03/12 SpikeMix = ERA 0511-12-02: 50 µl & Abs 051512: 50 µl Pct Recovery = 33% Analysis Date = 11/07/12 SpikeMix = ERA 0507-12-04.1: 50 µl & ERA 0511-12-02: 50 µl Pct Recovery = 42% Analysis Date = 04/22/13 SpikeMix = ERA 0507-12-04.1: 50 µl & Restek A089631: 50 µl Pct Recovery = 46% Analysis Date = 04/03/13 SpikeMix = Spex Organics T1120525010: 50 µl & Restek A089631: 50 µl Pct Recovery = 48% Analysis Date = 02/22/13 SpikeMix = Restek A089631: 50 µl & Supelco LB92781: 50 µl Pct Recovery = 38% Analysis Date = 12/18/12 SpikeMix = ERA 0507-12-04.1: 50 µl & Restek A089631: 50 µl Pct Recovery = 56% Analysis Date = 03/27/12 SpikeMix = Crescent 162776: 100 µl Pct Recovery = 71% Analysis Date = 01/27/12 SpikeMix = Supelco LB77167: 100 µl Pct Recovery = 38% Analysis Date = 10/13/11 SpikeMix = Supelco LB77167: 100 µl Pct Recovery = 46% Analysis Date = 06/07/11 SpikeMix = Supelco LB77167: 100 µl Pct Recovery = 45% Analysis Date = 03/10/11 SpikeMix = Crescent 162776: 100 µl Pct Recovery = 56% Analysis Date = 06/23/11 SpikeMix = Crescent 162776: 100 µl Pct Recovery = 51% Analysis Date = 04/10/13 SpikeMix = ERA 0511-12-02: 25 µl & Supelco LB92781: 25 µl Pct Recovery = 56% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120525010: 25 µl & ERA 0511-12-02: 25 µl Pct Recovery = 52% Analysis Date = 08/31/12 SpikeMix = ERA 0511-12-02: 25 µl & Abs 051512: 25 µl Pct Recovery = 45% Analysis Date = 12/18/12 SpikeMix = Restek A089631: 25 µl & Supelco LB92781: 25 µl Pct Recovery = 48% Analysis Date = 04/14/14 SpikeMix = ERA 0415-13-01.1A: 50 µl & Abs 071513: 50 µl Pct Recovery = 52% Analysis Date = 03/14/14 SpikeMix = Supelco LB99393: 50 µl & Abs 060413: 50 µl & Abs 071513: 50 µl Pct Recovery = 42% Analysis Date = 03/05/14 SpikeMix = ERA 0415-13-01.1A: 50 µl & Abs 060413: 50 µl & Abs 071513: 50 µl Pct Recovery = 32% Analysis Date = 03/05/14 SpikeMix = Spex Organics T1130423008: 50 µl & Abs 071513: 50 µl Pct Recovery = 35% Analysis Date = 03/14/14 SpikeMix = ERA 0415-13-01.2A: 50 µl & Spex Organics T1130423008: 50 µl Pct Recovery = 27% Analysis Date = 08/09/13 SpikeMix = ERA 0415-13-01.2A: 50 µl & Spex Organics T1130423008: 50 µl Pct Recovery = 29% Analysis Date = 01/21/15 SpikeMix = ChemService 2561700: 60 µl & Spex Organics E1140505004: 60 µl Pct Recovery = 30% Analysis Date = 09/23/14 SpikeMix = Supelco LC06946: 60 µl & ChemService 2561700: 60 µl Pct Recovery = 57% Analysis Date = 05/06/14 SpikeMix = Abs 031014: 60 µl & ChemService 2561700: 60 µl Pct Recovery = 65% Analysis Date = 02/12/15 SpikeMix = Supelco LC06946: 60 µl & Abs 042114: 60 µl Pct Recovery = 51% Analysis Date = 08/26/14 SpikeMix = Abs 031014: 60 µl & Abs 042114: 60 µl Pct Recovery = 63% Analysis Date = 01/13/17 SpikeMix = Abs 052616: 30 µl & ChemService 5016200: 30 µl Pct Recovery = 44% Analysis Date = 09/14/15 SpikeMix = ERA 0601-15-04: 50 µl & ChemService 4073900: 50 µl Pct Recovery = 57% Analysis Date = 08/10/15 SpikeMix = ERA 0601-15-04: 50 µl & Crescent 04EE007: 50 µl Pct Recovery = 39% Analysis Date = 02/19/14 SpikeMix = Abs 050813: 20 µl & Abs 071513: 20 µl Pct Recovery = 45% Analysis Date = 01/23/14 SpikeMix = Supelco LB99393: 20 µl & ERA 0415-13-01.2A: 20 µl & Abs 060413: 20 µl Pct Recovery = 26% Analysis Date = 01/21/15 SpikeMix = Supelco LC06946: 30 µl & ChemService 2561700: 30 µl Pct Recovery = 35% Analysis Date = 07/28/14 SpikeMix = ERA 0227-14-07.2: 30 µl & ChemService 2561700: 30 µl Pct Recovery = 87% Analysis Date = 05/14/14 SpikeMix = Abs 031014: 30 µl & ChemService 2561700: 30 µl Pct Recovery = 54% Analysis Date = 11/05/14 SpikeMix = ERA 0227-14-07.2: 30 µl & Abs 042114: 30 µl Pct Recovery = 53% Analysis Date = 07/27/12 SpikeMix = Supelco LB77167: 25 µl Pct Recovery = 53% Analysis Date = 04/17/12 SpikeMix = Supelco LB77167: 25 µl Pct Recovery = 44% Analysis Date = 04/06/12 SpikeMix = Crescent 162776: 25 µl Pct Recovery = 54% Analysis Date = 04/04/12 SpikeMix = Supelco LB77167: 25 µl Pct Recovery = 46% Analysis Date = 11/17/11 SpikeMix = Crescent 162776: 25 µl Pct Recovery = 37% Analysis Date = 10/12/11 SpikeMix = Crescent 162776: 25 µl Pct Recovery = 70% Analysis Date = 09/29/11 SpikeMix = Supelco LB77167: 25 µl Pct Recovery = 54% Analysis Date = 07/25/11 SpikeMix = Crescent 162776: 25 µl Pct Recovery = 34% Analysis Date = 05/19/11 SpikeMix = Supelco LB77167: 25 µl Pct Recovery = 89% Analysis Date = 03/31/11 SpikeMix = Supelco LB77167: 25 µl Pct Recovery = 67% Analysis Date = 05/09/11 SpikeMix = Crescent 162776: 25 µl Pct Recovery = 51% Analysis Date = 01/13/17 Pct Recovery = 46% Analysis Date = 01/02/17 Pct Recovery = 46% Analysis Date = 01/02/17 Pct Recovery = 46% Analysis Date = 12/22/16 Pct Recovery = 46% Analysis Date = 12/22/16 Pct Recovery = 46% Analysis Date = 12/11/16 Pct Recovery = 46% Analysis Date = 12/11/16 Pct Recovery = 46% Analysis Date = 12/01/16 Pct Recovery = 46% Analysis Date = 12/01/16 Pct Recovery = 46% Analysis Date = 11/20/16 Pct Recovery = 46% Analysis Date = 11/20/16 Pct Recovery = 46% Analysis Date = 11/09/16 Pct Recovery = 46% Analysis Date = 11/09/16 Pct Recovery = 46% Analysis Date = 10/30/16 Pct Recovery = 46% Analysis Date = 10/30/16 Pct Recovery = 46% Analysis Date = 10/19/16 Pct Recovery = 46% Analysis Date = 10/19/16 Pct Recovery = 46% Analysis Date = 10/08/16 Pct Recovery = 46% Analysis Date = 10/08/16 Pct Recovery = 46% Analysis Date = 09/28/16 Pct Recovery = 46% Analysis Date = 09/28/16 Pct Recovery = 46% Analysis Date = 09/17/16 Pct Recovery = 46% Analysis Date = 09/17/16 Pct Recovery = 46% Analysis Date = 09/06/16 Pct Recovery = 46% Analysis Date = 09/06/16 Pct Recovery = 46% Analysis Date = 08/27/16 Pct Recovery = 46% Analysis Date = 08/27/16 Pct Recovery = 46% Analysis Date = 08/16/16 Pct Recovery = 46% Analysis Date = 08/16/16 Pct Recovery = 46% Analysis Date = 08/05/16 Pct Recovery = 46% Analysis Date = 08/05/16 Pct Recovery = 46% Analysis Date = 07/26/16 Pct Recovery = 46% Analysis Date = 07/26/16 Pct Recovery = 46% Analysis Date = 07/15/16 Pct Recovery = 46% Analysis Date = 07/15/16 Pct Recovery = 46% Analysis Date = 07/04/16 Pct Recovery = 46% Analysis Date = 07/04/16 Pct Recovery = 46% Analysis Date = 06/24/16 Pct Recovery = 47% Analysis Date = 06/24/16 Pct Recovery = 47% Analysis Date = 06/13/16 Pct Recovery = 47% Analysis Date = 06/13/16 Pct Recovery = 47% Analysis Date = 06/02/16 Pct Recovery = 47% Analysis Date = 06/02/16 Pct Recovery = 47% Analysis Date = 05/23/16 Pct Recovery = 47% Analysis Date = 05/23/16 Pct Recovery = 47% Analysis Date = 05/12/16 Pct Recovery = 47% Analysis Date = 05/12/16 Pct Recovery = 47% Analysis Date = 05/01/16 Pct Recovery = 47% Analysis Date = 05/01/16 Pct Recovery = 47% Analysis Date = 04/21/16 Pct Recovery = 47% Analysis Date = 04/21/16 Pct Recovery = 47% Analysis Date = 04/10/16 Pct Recovery = 47% Analysis Date = 04/10/16 Pct Recovery = 47% Analysis Date = 03/30/16 Pct Recovery = 47% Analysis Date = 03/30/16 Pct Recovery = 47% Analysis Date = 03/19/16 Pct Recovery = 47% Analysis Date = 03/19/16 Pct Recovery = 47% Analysis Date = 03/09/16 Pct Recovery = 47% Analysis Date = 03/09/16 Pct Recovery = 47% Analysis Date = 02/27/16 Pct Recovery = 47% Analysis Date = 02/27/16 Pct Recovery = 47% Analysis Date = 02/16/16 Pct Recovery = 47% Analysis Date = 02/16/16 Pct Recovery = 47% Analysis Date = 02/06/16 Pct Recovery = 47% Analysis Date = 02/06/16 Pct Recovery = 47% Analysis Date = 01/26/16 Pct Recovery = 47% Analysis Date = 01/26/16 Pct Recovery = 47% Analysis Date = 01/15/16 Pct Recovery = 47% Analysis Date = 01/15/16 Pct Recovery = 47% Analysis Date = 01/05/16 Pct Recovery = 47% Analysis Date = 01/05/16 Pct Recovery = 47% Analysis Date = 12/25/15 Pct Recovery = 47% Analysis Date = 12/25/15 Pct Recovery = 47% Analysis Date = 12/14/15 Pct Recovery = 47% Analysis Date = 12/14/15 Pct Recovery = 47% Analysis Date = 12/04/15 Pct Recovery = 47% Analysis Date = 12/04/15 Pct Recovery = 47% Analysis Date = 11/23/15 Pct Recovery = 47% Analysis Date = 11/23/15 Pct Recovery = 47% Analysis Date = 11/12/15 Pct Recovery = 47% Analysis Date = 11/12/15 Pct Recovery = 47% Analysis Date = 11/02/15 Pct Recovery = 47% Analysis Date = 11/02/15 Pct Recovery = 47% Analysis Date = 10/22/15 Pct Recovery = 47% Analysis Date = 10/22/15 Pct Recovery = 47% Analysis Date = 10/11/15 Pct Recovery = 47% Analysis Date = 10/11/15 Pct Recovery = 47% Analysis Date = 10/01/15 Pct Recovery = 47% Analysis Date = 10/01/15 Pct Recovery = 47% Analysis Date = 09/20/15 Pct Recovery = 47% Analysis Date = 09/20/15 Pct Recovery = 47% Analysis Date = 09/09/15 Pct Recovery = 48% Analysis Date = 09/09/15 Pct Recovery = 48% Analysis Date = 08/30/15 Pct Recovery = 48% Analysis Date = 08/30/15 Pct Recovery = 48% Analysis Date = 08/19/15 Pct Recovery = 48% Analysis Date = 08/19/15 Pct Recovery = 48% Analysis Date = 08/08/15 Pct Recovery = 48% Analysis Date = 08/08/15 Pct Recovery = 48% Analysis Date = 07/29/15 Pct Recovery = 48% Analysis Date = 07/29/15 Pct Recovery = 48% Analysis Date = 07/18/15 Pct Recovery = 48% Analysis Date = 07/18/15 Pct Recovery = 48% Analysis Date = 07/07/15 Pct Recovery = 48% Analysis Date = 07/07/15 Pct Recovery = 48% Analysis Date = 06/26/15 Pct Recovery = 48% Analysis Date = 06/26/15 Pct Recovery = 48% Analysis Date = 06/16/15 Pct Recovery = 48% Analysis Date = 06/16/15 Pct Recovery = 48% Analysis Date = 06/05/15 Pct Recovery = 48% Analysis Date = 06/05/15 Pct Recovery = 48% Analysis Date = 05/25/15 Pct Recovery = 48% Analysis Date = 05/25/15 Pct Recovery = 48% Analysis Date = 05/15/15 Pct Recovery = 48% Analysis Date = 05/15/15 Pct Recovery = 48% Analysis Date = 05/04/15 Pct Recovery = 48% Analysis Date = 05/04/15 Pct Recovery = 48% Analysis Date = 04/23/15 Pct Recovery = 48% Analysis Date = 04/23/15 Pct Recovery = 48% Analysis Date = 04/13/15 Pct Recovery = 48% Analysis Date = 04/13/15 Pct Recovery = 48% Analysis Date = 04/02/15 Pct Recovery = 48% Analysis Date = 04/02/15 Pct Recovery = 48% Analysis Date = 03/22/15 Pct Recovery = 48% Analysis Date = 03/22/15 Pct Recovery = 48% Analysis Date = 03/12/15 Pct Recovery = 48% Analysis Date = 03/12/15 Pct Recovery = 48% Analysis Date = 03/01/15 Pct Recovery = 48% Analysis Date = 03/01/15 Pct Recovery = 48% Analysis Date = 02/18/15 Pct Recovery = 48% Analysis Date = 02/18/15 Pct Recovery = 48% Analysis Date = 02/08/15 Pct Recovery = 48% Analysis Date = 02/08/15 Pct Recovery = 48% Analysis Date = 01/28/15 Pct Recovery = 48% Analysis Date = 01/28/15 Pct Recovery = 48% Analysis Date = 01/17/15 Pct Recovery = 48% Analysis Date = 01/17/15 Pct Recovery = 48% Analysis Date = 01/07/15 Pct Recovery = 48% Analysis Date = 01/07/15 Pct Recovery = 48% Analysis Date = 12/27/14 Pct Recovery = 48% Analysis Date = 12/27/14 Pct Recovery = 48% Analysis Date = 12/16/14 Pct Recovery = 48% Analysis Date = 12/16/14 Pct Recovery = 48% Analysis Date = 12/06/14 Pct Recovery = 48% Analysis Date = 12/06/14 Pct Recovery = 48% Analysis Date = 11/25/14 Pct Recovery = 48% Analysis Date = 11/25/14 Pct Recovery = 48% Analysis Date = 11/14/14 Pct Recovery = 48% Analysis Date = 11/14/14 Pct Recovery = 48% Analysis Date = 11/04/14 Pct Recovery = 48% Analysis Date = 11/04/14 Pct Recovery = 48% Analysis Date = 10/24/14 Pct Recovery = 48% Analysis Date = 10/24/14 Pct Recovery = 48% Analysis Date = 10/13/14 Pct Recovery = 48% Analysis Date = 10/13/14 Pct Recovery = 48% Analysis Date = 10/02/14 Pct Recovery = 48% Analysis Date = 10/02/14 Pct Recovery = 48% Analysis Date = 09/22/14 Pct Recovery = 48% Analysis Date = 09/22/14 Pct Recovery = 48% Analysis Date = 09/11/14 Pct Recovery = 48% Analysis Date = 09/11/14 Pct Recovery = 48% Analysis Date = 08/31/14 Pct Recovery = 48% Analysis Date = 08/31/14 Pct Recovery = 48% Analysis Date = 08/21/14 Pct Recovery = 48% Analysis Date = 08/21/14 Pct Recovery = 48% Analysis Date = 08/10/14 Pct Recovery = 47% Analysis Date = 08/10/14 Pct Recovery = 47% Analysis Date = 07/30/14 Pct Recovery = 47% Analysis Date = 07/30/14 Pct Recovery = 47% Analysis Date = 07/20/14 Pct Recovery = 47% Analysis Date = 07/20/14 Pct Recovery = 47% Analysis Date = 07/09/14 Pct Recovery = 47% Analysis Date = 07/09/14 Pct Recovery = 47% Analysis Date = 06/28/14 Pct Recovery = 47% Analysis Date = 06/28/14 Pct Recovery = 47% Analysis Date = 06/18/14 Pct Recovery = 47% Analysis Date = 06/18/14 Pct Recovery = 47% Analysis Date = 06/07/14 Pct Recovery = 47% Analysis Date = 06/07/14 Pct Recovery = 47% Analysis Date = 05/27/14 Pct Recovery = 47% Analysis Date = 05/27/14 Pct Recovery = 47% Analysis Date = 05/17/14 Pct Recovery = 47% Analysis Date = 05/17/14 Pct Recovery = 47% Analysis Date = 05/06/14 Pct Recovery = 47% Analysis Date = 05/06/14 Pct Recovery = 47% Analysis Date = 04/25/14 Pct Recovery = 47% Analysis Date = 04/25/14 Pct Recovery = 47% Analysis Date = 04/15/14 Pct Recovery = 47% Analysis Date = 04/15/14 Pct Recovery = 47% Analysis Date = 04/04/14 Pct Recovery = 47% Analysis Date = 04/04/14 Pct Recovery = 47% Analysis Date = 03/24/14 Pct Recovery = 47% Analysis Date = 03/24/14 Pct Recovery = 47% Analysis Date = 03/14/14 Pct Recovery = 47% Analysis Date = 03/14/14 Pct Recovery = 47% Analysis Date = 03/03/14 Pct Recovery = 47% Analysis Date = 03/03/14 Pct Recovery = 47% Analysis Date = 02/20/14 Pct Recovery = 47% Analysis Date = 02/20/14 Pct Recovery = 47% Analysis Date = 02/10/14 Pct Recovery = 47% Analysis Date = 02/10/14 Pct Recovery = 47% Analysis Date = 01/30/14 Pct Recovery = 47% Analysis Date = 01/30/14 Pct Recovery = 47% Analysis Date = 01/19/14 Pct Recovery = 46% Analysis Date = 01/19/14 Pct Recovery = 46% Analysis Date = 01/08/14 Pct Recovery = 46% Analysis Date = 01/08/14 Pct Recovery = 46% Analysis Date = 12/29/13 Pct Recovery = 46% Analysis Date = 12/29/13 Pct Recovery = 46% Analysis Date = 12/18/13 Pct Recovery = 46% Analysis Date = 12/18/13 Pct Recovery = 46% Analysis Date = 12/07/13 Pct Recovery = 46% Analysis Date = 12/07/13 Pct Recovery = 46% Analysis Date = 11/27/13 Pct Recovery = 46% Analysis Date = 11/27/13 Pct Recovery = 46% Analysis Date = 11/16/13 Pct Recovery = 46% Analysis Date = 11/16/13 Pct Recovery = 46% Analysis Date = 11/05/13 Pct Recovery = 46% Analysis Date = 11/05/13 Pct Recovery = 46% Analysis Date = 10/26/13 Pct Recovery = 46% Analysis Date = 10/26/13 Pct Recovery = 46% Analysis Date = 10/15/13 Pct Recovery = 46% Analysis Date = 10/15/13 Pct Recovery = 46% Analysis Date = 10/04/13 Pct Recovery = 46% Analysis Date = 10/04/13 Pct Recovery = 46% Analysis Date = 09/24/13 Pct Recovery = 46% Analysis Date = 09/24/13 Pct Recovery = 46% Analysis Date = 09/13/13 Pct Recovery = 46% Analysis Date = 09/13/13 Pct Recovery = 46% Analysis Date = 09/02/13 Pct Recovery = 46% Analysis Date = 09/02/13 Pct Recovery = 46% Analysis Date = 08/23/13 Pct Recovery = 45% Analysis Date = 08/23/13 Pct Recovery = 45% Analysis Date = 08/12/13 Pct Recovery = 45% Analysis Date = 08/12/13 Pct Recovery = 45% Analysis Date = 08/01/13 Pct Recovery = 45% Analysis Date = 08/01/13 Pct Recovery = 45% Analysis Date = 07/22/13 Pct Recovery = 45% Analysis Date = 07/22/13 Pct Recovery = 45% Analysis Date = 07/11/13 Pct Recovery = 45% Analysis Date = 07/11/13 Pct Recovery = 45% Analysis Date = 06/30/13 Pct Recovery = 45% Analysis Date = 06/30/13 Pct Recovery = 45% Analysis Date = 06/20/13 Pct Recovery = 45% Analysis Date = 06/20/13 Pct Recovery = 45% Analysis Date = 06/09/13 Pct Recovery = 45% Analysis Date = 06/09/13 Pct Recovery = 45% Analysis Date = 05/29/13 Pct Recovery = 45% Analysis Date = 05/29/13 Pct Recovery = 45% Analysis Date = 05/19/13 Pct Recovery = 45% Analysis Date = 05/19/13 Pct Recovery = 45% Analysis Date = 05/08/13 Pct Recovery = 45% Analysis Date = 05/08/13 Pct Recovery = 45% Analysis Date = 04/27/13 Pct Recovery = 45% Analysis Date = 04/27/13 Pct Recovery = 45% Analysis Date = 04/16/13 Pct Recovery = 45% Analysis Date = 04/16/13 Pct Recovery = 45% Analysis Date = 04/06/13 Pct Recovery = 45% Analysis Date = 04/06/13 Pct Recovery = 45% Analysis Date = 03/26/13 Pct Recovery = 45% Analysis Date = 03/26/13 Pct Recovery = 45% Analysis Date = 03/15/13 Pct Recovery = 45% Analysis Date = 03/15/13 Pct Recovery = 45% Analysis Date = 03/05/13 Pct Recovery = 45% Analysis Date = 03/05/13 Pct Recovery = 45% Analysis Date = 02/22/13 Pct Recovery = 45% Analysis Date = 02/22/13 Pct Recovery = 45% Analysis Date = 02/11/13 Pct Recovery = 45% Analysis Date = 02/11/13 Pct Recovery = 45% Analysis Date = 02/01/13 Pct Recovery = 45% Analysis Date = 02/01/13 Pct Recovery = 45% Analysis Date = 01/21/13 Pct Recovery = 46% Analysis Date = 01/21/13 Pct Recovery = 46% Analysis Date = 01/10/13 Pct Recovery = 46% Analysis Date = 01/10/13 Pct Recovery = 46% Analysis Date = 12/31/12 Pct Recovery = 46% Analysis Date = 12/31/12 Pct Recovery = 46% Analysis Date = 12/20/12 Pct Recovery = 46% Analysis Date = 12/20/12 Pct Recovery = 46% Analysis Date = 12/09/12 Pct Recovery = 46% Analysis Date = 12/09/12 Pct Recovery = 46% Analysis Date = 11/29/12 Pct Recovery = 47% Analysis Date = 11/29/12 Pct Recovery = 47% Analysis Date = 11/18/12 Pct Recovery = 47% Analysis Date = 11/18/12 Pct Recovery = 47% Analysis Date = 11/07/12 Pct Recovery = 47% Analysis Date = 11/07/12 Pct Recovery = 47% Analysis Date = 10/28/12 Pct Recovery = 47% Analysis Date = 10/28/12 Pct Recovery = 47% Analysis Date = 10/17/12 Pct Recovery = 47% Analysis Date = 10/17/12 Pct Recovery = 47% Analysis Date = 10/06/12 Pct Recovery = 47% Analysis Date = 10/06/12 Pct Recovery = 47% Analysis Date = 09/26/12 Pct Recovery = 47% Analysis Date = 09/26/12 Pct Recovery = 47% Analysis Date = 09/15/12 Pct Recovery = 48% Analysis Date = 09/15/12 Pct Recovery = 48% Analysis Date = 09/04/12 Pct Recovery = 48% Analysis Date = 09/04/12 Pct Recovery = 48% Analysis Date = 08/25/12 Pct Recovery = 48% Analysis Date = 08/25/12 Pct Recovery = 48% Analysis Date = 08/14/12 Pct Recovery = 48% Analysis Date = 08/14/12 Pct Recovery = 48% Analysis Date = 08/03/12 Pct Recovery = 48% Analysis Date = 08/03/12 Pct Recovery = 48% Analysis Date = 07/23/12 Pct Recovery = 48% Analysis Date = 07/23/12 Pct Recovery = 48% Analysis Date = 07/13/12 Pct Recovery = 49% Analysis Date = 07/13/12 Pct Recovery = 49% Analysis Date = 07/02/12 Pct Recovery = 49% Analysis Date = 07/02/12 Pct Recovery = 49% Analysis Date = 06/21/12 Pct Recovery = 49% Analysis Date = 06/21/12 Pct Recovery = 49% Analysis Date = 06/11/12 Pct Recovery = 49% Analysis Date = 06/11/12 Pct Recovery = 49% Analysis Date = 05/31/12 Pct Recovery = 49% Analysis Date = 05/31/12 Pct Recovery = 49% Analysis Date = 05/20/12 Pct Recovery = 49% Analysis Date = 05/20/12 Pct Recovery = 49% Analysis Date = 05/10/12 Pct Recovery = 50% Analysis Date = 05/10/12 Pct Recovery = 50% Analysis Date = 04/29/12 Pct Recovery = 50% Analysis Date = 04/29/12 Pct Recovery = 50% Analysis Date = 04/18/12 Pct Recovery = 50% Analysis Date = 04/18/12 Pct Recovery = 50% Analysis Date = 04/08/12 Pct Recovery = 50% Analysis Date = 04/08/12 Pct Recovery = 50% Analysis Date = 03/28/12 Pct Recovery = 50% Analysis Date = 03/28/12 Pct Recovery = 50% Analysis Date = 03/17/12 Pct Recovery = 50% Analysis Date = 03/17/12 Pct Recovery = 50% Analysis Date = 03/07/12 Pct Recovery = 51% Analysis Date = 03/07/12 Pct Recovery = 51% Analysis Date = 02/25/12 Pct Recovery = 51% Analysis Date = 02/25/12 Pct Recovery = 51% Analysis Date = 02/14/12 Pct Recovery = 51% Analysis Date = 02/14/12 Pct Recovery = 51% Analysis Date = 02/04/12 Pct Recovery = 51% Analysis Date = 02/04/12 Pct Recovery = 51% Analysis Date = 01/24/12 Pct Recovery = 51% Analysis Date = 01/24/12 Pct Recovery = 51% Analysis Date = 01/13/12 Pct Recovery = 52% Analysis Date = 01/13/12 Pct Recovery = 52% Analysis Date = 01/03/12 Pct Recovery = 52% Analysis Date = 01/03/12 Pct Recovery = 52% Analysis Date = 12/23/11 Pct Recovery = 52% Analysis Date = 12/23/11 Pct Recovery = 52% Analysis Date = 12/12/11 Pct Recovery = 52% Analysis Date = 12/12/11 Pct Recovery = 52% Analysis Date = 12/02/11 Pct Recovery = 52% Analysis Date = 12/02/11 Pct Recovery = 52% Analysis Date = 11/21/11 Pct Recovery = 52% Analysis Date = 11/21/11 Pct Recovery = 52% Analysis Date = 11/10/11 Pct Recovery = 53% Analysis Date = 11/10/11 Pct Recovery = 53% Analysis Date = 10/30/11 Pct Recovery = 53% Analysis Date = 10/30/11 Pct Recovery = 53% Analysis Date = 10/20/11 Pct Recovery = 53% Analysis Date = 10/20/11 Pct Recovery = 53% Analysis Date = 10/09/11 Pct Recovery = 53% Analysis Date = 10/09/11 Pct Recovery = 53% Analysis Date = 09/28/11 Pct Recovery = 53% Analysis Date = 09/28/11 Pct Recovery = 53% Analysis Date = 09/18/11 Pct Recovery = 54% Analysis Date = 09/18/11 Pct Recovery = 54% Analysis Date = 09/07/11 Pct Recovery = 54% Analysis Date = 09/07/11 Pct Recovery = 54% Analysis Date = 08/27/11 Pct Recovery = 54% Analysis Date = 08/27/11 Pct Recovery = 54% Analysis Date = 08/17/11 Pct Recovery = 54% Analysis Date = 08/17/11 Pct Recovery = 54% Analysis Date = 08/06/11 Pct Recovery = 54% Analysis Date = 08/06/11 Pct Recovery = 54% Analysis Date = 07/26/11 Pct Recovery = 55% Analysis Date = 07/26/11 Pct Recovery = 55% Analysis Date = 07/16/11 Pct Recovery = 55% Analysis Date = 07/16/11 Pct Recovery = 55% Analysis Date = 07/05/11 Pct Recovery = 55% Analysis Date = 07/05/11 Pct Recovery = 55% Analysis Date = 06/24/11 Pct Recovery = 55% Analysis Date = 06/24/11 Pct Recovery = 55% Analysis Date = 06/14/11 Pct Recovery = 55% Analysis Date = 06/14/11 Pct Recovery = 55% Analysis Date = 06/03/11 Pct Recovery = 56% Analysis Date = 06/03/11 Pct Recovery = 56% Analysis Date = 05/23/11 Pct Recovery = 56% Analysis Date = 05/23/11 Pct Recovery = 56% Analysis Date = 05/13/11 Pct Recovery = 56% Analysis Date = 05/13/11 Pct Recovery = 56% Analysis Date = 05/02/11 Pct Recovery = 56% Analysis Date = 05/02/11 Pct Recovery = 56% Analysis Date = 04/21/11 Pct Recovery = 56% Analysis Date = 04/21/11 Pct Recovery = 56% Analysis Date = 04/11/11 Pct Recovery = 56% Analysis Date = 04/11/11 Pct Recovery = 56% Analysis Date = 03/31/11 Pct Recovery = 57% Analysis Date = 03/31/11 Pct Recovery = 57% Analysis Date = 03/20/11 Pct Recovery = 57% Analysis Date = 03/20/11 Pct Recovery = 57% Analysis Date = 03/10/11 Pct Recovery = 57% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
MESTRANOL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 50 49% 14% 48% 12%
Total 50 49% 14% 48% 12%

Sample Statistics
MESTRANOL

Characteristic N % % Basis
Plotted 50 63% Spiked
Estimated Values 2 3% Spiked
Deleted Values 2 2% Spiked + Not Spiked
Spiked, Censored 2 3% Spiked
Spiked 81 .  
False Negatives 28 35% 28 out of 80
Not Spiked 50 .  
False Positives 2 4% 2 out of 49

BQS OBSP Determination:
NORETHINDRONE
METHOD: 4434 , TESTIDCODE: 64531GM005
Open Data Set

Analysis Date = 04/22/13 SpikeMix = ERA 0507-12-04.1: 50 µl & Restek A089631: 50 µl Pct Recovery = 72% Analysis Date = 12/18/12 SpikeMix = ERA 0507-12-04.1: 50 µl & Restek A089631: 50 µl Pct Recovery = 66% Analysis Date = 11/07/12 SpikeMix = ERA 0507-12-04.1: 50 µl & ERA 0511-12-02: 50 µl Pct Recovery = 73% Analysis Date = 04/03/13 SpikeMix = Spex Organics T1120525010: 50 µl & Restek A089631: 50 µl Pct Recovery = 70% Analysis Date = 12/18/12 SpikeMix = Spex Organics T1120525010: 50 µl & Supelco LB92781: 50 µl Pct Recovery = 70% Analysis Date = 02/08/13 SpikeMix = ERA 0507-12-04.1: 25 µl & Supelco LB92781: 25 µl Pct Recovery = 70% Analysis Date = 11/01/12 SpikeMix = ERA 0507-12-04.1: 25 µl & Abs 051512: 25 µl Pct Recovery = 63% Analysis Date = 04/03/13 SpikeMix = Spex Organics T1120525010: 25 µl & Abs 051512: 25 µl Pct Recovery = 62% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120525010: 25 µl & ERA 0511-12-02: 25 µl Pct Recovery = 78% Analysis Date = 08/29/12 SpikeMix = Spex Organics T1120525010: 25 µl Pct Recovery = 83% Analysis Date = 03/27/12 SpikeMix = Crescent 162776: 100 µl Pct Recovery = 85% Analysis Date = 01/27/12 SpikeMix = Supelco LB77167: 100 µl Pct Recovery = 68% Analysis Date = 10/13/11 SpikeMix = Supelco LB77167: 100 µl Pct Recovery = 76% Analysis Date = 06/07/11 SpikeMix = Supelco LB77167: 100 µl Pct Recovery = 77% Analysis Date = 03/10/11 SpikeMix = Crescent 162776: 100 µl Pct Recovery = 65% Analysis Date = 06/23/11 SpikeMix = Crescent 162776: 100 µl Pct Recovery = 67% Analysis Date = 04/14/14 SpikeMix = ERA 0415-13-01.1A: 50 µl & Abs 071513: 50 µl Pct Recovery = 90% Analysis Date = 03/14/14 SpikeMix = Supelco LB99393: 50 µl & Abs 050813: 50 µl Pct Recovery = 82% Analysis Date = 03/14/14 SpikeMix = Supelco LB99393: 50 µl & Abs 060413: 50 µl & Abs 071513: 50 µl Pct Recovery = 67% Analysis Date = 03/05/14 SpikeMix = ERA 0415-13-01.1A: 50 µl & Abs 060413: 50 µl & Abs 071513: 50 µl Pct Recovery = 69% Analysis Date = 02/25/14 SpikeMix = ERA 0415-13-01.1A: 50 µl & Abs 050813: 50 µl Pct Recovery = 58% Analysis Date = 08/19/16 SpikeMix = Supelco LC20140V: 50 µl & Spex Organics TS160420010: 50 µl Pct Recovery = 98% Analysis Date = 12/15/16 SpikeMix = Abs 061416H: 50 µl & ChemService 5016100: 50 µl Pct Recovery = 80% Analysis Date = 04/13/15 SpikeMix = Abs 042114: 60 µl & Spex Organics E1140505004: 60 µl Pct Recovery = 84% Analysis Date = 04/01/15 SpikeMix = Spex Organics E1140505004: 60 µl & Supelco LC06946: 60 µl Pct Recovery = 73% Analysis Date = 01/21/15 SpikeMix = ChemService 2561700: 60 µl & Spex Organics E1140505004: 60 µl Pct Recovery = 76% Analysis Date = 12/09/14 SpikeMix = Abs 031014: 60 µl & Supelco LC06946: 60 µl Pct Recovery = 81% Analysis Date = 08/26/14 SpikeMix = Abs 031014: 60 µl & Abs 042114: 60 µl Pct Recovery = 89% Analysis Date = 08/11/14 SpikeMix = Abs 031014: 60 µl & ERA 0227-14-07.2: 60 µl Pct Recovery = 110% Analysis Date = 05/06/14 SpikeMix = Abs 031014: 60 µl & ChemService 2561700: 60 µl Pct Recovery = 136% Analysis Date = 01/07/16 SpikeMix = Crescent 04EE007: 60 µl & Abs 041515: 60 µl Pct Recovery = 100% Analysis Date = 02/01/17 SpikeMix = Supelco LC20140V: 30 µl & Abs 052616: 30 µl Pct Recovery = 89% Analysis Date = 12/29/16 SpikeMix = ChemService 5016100: 30 µl & Abs 052616: 30 µl Pct Recovery = 94% Analysis Date = 09/21/16 SpikeMix = ChemService 5016200: 30 µl & ChemService 5016100: 30 µl Pct Recovery = 65% Analysis Date = 12/10/15 SpikeMix = Abs 041515: 50 µl & ERA 0601-15-04: 50 µl Pct Recovery = 82% Analysis Date = 08/17/15 SpikeMix = ChemService 4073900: 50 µl & Abs 041515: 50 µl Pct Recovery = 84% Analysis Date = 06/24/16 SpikeMix = Crescent 04EE007: 50 µl & Spex Organics EN150501025: 50 µl Pct Recovery = 145% Analysis Date = 01/23/14 SpikeMix = Supelco LB99393: 20 µl & ERA 0415-13-01.2A: 20 µl & Abs 060413: 20 µl Pct Recovery = 68% Analysis Date = 12/09/13 SpikeMix = Supelco LB99393: 20 µl & Spex Organics T1130423008: 20 µl Pct Recovery = 52% Analysis Date = 09/16/13 SpikeMix = ERA 0415-13-01.1A: 20 µl & ERA 0415-13-01.2A: 20 µl & Abs 060413: 20 µl Pct Recovery = 72% Analysis Date = 07/19/13 SpikeMix = Supelco LB99393: 20 µl & ERA 0415-13-01.2A: 20 µl Pct Recovery = 67% Analysis Date = 06/27/13 SpikeMix = ERA 0415-13-01.1A: 20 µl & Spex Organics T1130423008: 20 µl Pct Recovery = 79% Analysis Date = 06/04/13 SpikeMix = Supelco LB99393: 20 µl & Spex Organics T1130423008: 20 µl Pct Recovery = 51% Analysis Date = 06/03/15 SpikeMix = Abs 031014: 30 µl & ERA 0227-14-07.2: 30 µl Pct Recovery = 90% Analysis Date = 04/01/15 SpikeMix = ChemService 2561700: 30 µl & Spex Organics E1140505004: 30 µl Pct Recovery = 105% Analysis Date = 01/29/15 SpikeMix = Abs 031014: 30 µl & Supelco LC06946: 30 µl Pct Recovery = 71% Analysis Date = 12/23/14 SpikeMix = Spex Organics E1140505004: 30 µl & Supelco LC06946: 30 µl Pct Recovery = 94% Analysis Date = 07/14/14 SpikeMix = ERA 0227-14-07.2: 30 µl & Abs 031014: 30 µl Pct Recovery = 61% Analysis Date = 05/14/14 SpikeMix = Abs 031014: 30 µl & ChemService 2561700: 30 µl Pct Recovery = 103% Analysis Date = 07/27/12 SpikeMix = Supelco LB77167: 25 µl Pct Recovery = 66% Analysis Date = 04/17/12 SpikeMix = Supelco LB77167: 25 µl Pct Recovery = 82% Analysis Date = 04/06/12 SpikeMix = Crescent 162776: 25 µl Pct Recovery = 74% Analysis Date = 04/04/12 SpikeMix = Supelco LB77167: 25 µl Pct Recovery = 94% Analysis Date = 11/17/11 SpikeMix = Crescent 162776: 25 µl Pct Recovery = 75% Analysis Date = 07/25/11 SpikeMix = Crescent 162776: 25 µl Pct Recovery = 56% Analysis Date = 05/19/11 SpikeMix = Supelco LB77167: 25 µl Pct Recovery = 95% Analysis Date = 03/31/11 SpikeMix = Supelco LB77167: 25 µl Pct Recovery = 63% Analysis Date = 05/09/11 SpikeMix = Crescent 162776: 25 µl Pct Recovery = 64% Analysis Date = 02/01/17 Pct Recovery = 94% Analysis Date = 01/21/17 Pct Recovery = 94% Analysis Date = 01/21/17 Pct Recovery = 94% Analysis Date = 01/10/17 Pct Recovery = 94% Analysis Date = 01/10/17 Pct Recovery = 94% Analysis Date = 12/30/16 Pct Recovery = 94% Analysis Date = 12/30/16 Pct Recovery = 94% Analysis Date = 12/19/16 Pct Recovery = 94% Analysis Date = 12/19/16 Pct Recovery = 94% Analysis Date = 12/09/16 Pct Recovery = 94% Analysis Date = 12/09/16 Pct Recovery = 94% Analysis Date = 11/28/16 Pct Recovery = 94% Analysis Date = 11/28/16 Pct Recovery = 94% Analysis Date = 11/17/16 Pct Recovery = 94% Analysis Date = 11/17/16 Pct Recovery = 94% Analysis Date = 11/06/16 Pct Recovery = 93% Analysis Date = 11/06/16 Pct Recovery = 93% Analysis Date = 10/27/16 Pct Recovery = 93% Analysis Date = 10/27/16 Pct Recovery = 93% Analysis Date = 10/16/16 Pct Recovery = 93% Analysis Date = 10/16/16 Pct Recovery = 93% Analysis Date = 10/05/16 Pct Recovery = 93% Analysis Date = 10/05/16 Pct Recovery = 93% Analysis Date = 09/24/16 Pct Recovery = 93% Analysis Date = 09/24/16 Pct Recovery = 93% Analysis Date = 09/13/16 Pct Recovery = 93% Analysis Date = 09/13/16 Pct Recovery = 93% Analysis Date = 09/03/16 Pct Recovery = 93% Analysis Date = 09/03/16 Pct Recovery = 93% Analysis Date = 08/23/16 Pct Recovery = 93% Analysis Date = 08/23/16 Pct Recovery = 93% Analysis Date = 08/12/16 Pct Recovery = 93% Analysis Date = 08/12/16 Pct Recovery = 93% Analysis Date = 08/01/16 Pct Recovery = 93% Analysis Date = 08/01/16 Pct Recovery = 93% Analysis Date = 07/22/16 Pct Recovery = 92% Analysis Date = 07/22/16 Pct Recovery = 92% Analysis Date = 07/11/16 Pct Recovery = 92% Analysis Date = 07/11/16 Pct Recovery = 92% Analysis Date = 06/30/16 Pct Recovery = 92% Analysis Date = 06/30/16 Pct Recovery = 92% Analysis Date = 06/19/16 Pct Recovery = 92% Analysis Date = 06/19/16 Pct Recovery = 92% Analysis Date = 06/08/16 Pct Recovery = 92% Analysis Date = 06/08/16 Pct Recovery = 92% Analysis Date = 05/29/16 Pct Recovery = 92% Analysis Date = 05/29/16 Pct Recovery = 92% Analysis Date = 05/18/16 Pct Recovery = 92% Analysis Date = 05/18/16 Pct Recovery = 92% Analysis Date = 05/07/16 Pct Recovery = 92% Analysis Date = 05/07/16 Pct Recovery = 92% Analysis Date = 04/26/16 Pct Recovery = 92% Analysis Date = 04/26/16 Pct Recovery = 92% Analysis Date = 04/16/16 Pct Recovery = 92% Analysis Date = 04/16/16 Pct Recovery = 92% Analysis Date = 04/05/16 Pct Recovery = 91% Analysis Date = 04/05/16 Pct Recovery = 91% Analysis Date = 03/25/16 Pct Recovery = 91% Analysis Date = 03/25/16 Pct Recovery = 91% Analysis Date = 03/14/16 Pct Recovery = 91% Analysis Date = 03/14/16 Pct Recovery = 91% Analysis Date = 03/03/16 Pct Recovery = 91% Analysis Date = 03/03/16 Pct Recovery = 91% Analysis Date = 02/22/16 Pct Recovery = 91% Analysis Date = 02/22/16 Pct Recovery = 91% Analysis Date = 02/11/16 Pct Recovery = 91% Analysis Date = 02/11/16 Pct Recovery = 91% Analysis Date = 01/31/16 Pct Recovery = 91% Analysis Date = 01/31/16 Pct Recovery = 91% Analysis Date = 01/20/16 Pct Recovery = 91% Analysis Date = 01/20/16 Pct Recovery = 91% Analysis Date = 01/10/16 Pct Recovery = 91% Analysis Date = 01/10/16 Pct Recovery = 91% Analysis Date = 12/30/15 Pct Recovery = 91% Analysis Date = 12/30/15 Pct Recovery = 91% Analysis Date = 12/19/15 Pct Recovery = 90% Analysis Date = 12/19/15 Pct Recovery = 90% Analysis Date = 12/08/15 Pct Recovery = 90% Analysis Date = 12/08/15 Pct Recovery = 90% Analysis Date = 11/28/15 Pct Recovery = 90% Analysis Date = 11/28/15 Pct Recovery = 90% Analysis Date = 11/17/15 Pct Recovery = 90% Analysis Date = 11/17/15 Pct Recovery = 90% Analysis Date = 11/06/15 Pct Recovery = 90% Analysis Date = 11/06/15 Pct Recovery = 90% Analysis Date = 10/26/15 Pct Recovery = 90% Analysis Date = 10/26/15 Pct Recovery = 90% Analysis Date = 10/15/15 Pct Recovery = 90% Analysis Date = 10/15/15 Pct Recovery = 90% Analysis Date = 10/05/15 Pct Recovery = 90% Analysis Date = 10/05/15 Pct Recovery = 90% Analysis Date = 09/24/15 Pct Recovery = 90% Analysis Date = 09/24/15 Pct Recovery = 90% Analysis Date = 09/13/15 Pct Recovery = 90% Analysis Date = 09/13/15 Pct Recovery = 90% Analysis Date = 09/02/15 Pct Recovery = 90% Analysis Date = 09/02/15 Pct Recovery = 90% Analysis Date = 08/23/15 Pct Recovery = 90% Analysis Date = 08/23/15 Pct Recovery = 90% Analysis Date = 08/12/15 Pct Recovery = 89% Analysis Date = 08/12/15 Pct Recovery = 89% Analysis Date = 08/01/15 Pct Recovery = 89% Analysis Date = 08/01/15 Pct Recovery = 89% Analysis Date = 07/21/15 Pct Recovery = 89% Analysis Date = 07/21/15 Pct Recovery = 89% Analysis Date = 07/10/15 Pct Recovery = 89% Analysis Date = 07/10/15 Pct Recovery = 89% Analysis Date = 06/30/15 Pct Recovery = 89% Analysis Date = 06/30/15 Pct Recovery = 89% Analysis Date = 06/19/15 Pct Recovery = 89% Analysis Date = 06/19/15 Pct Recovery = 89% Analysis Date = 06/08/15 Pct Recovery = 89% Analysis Date = 06/08/15 Pct Recovery = 89% Analysis Date = 05/28/15 Pct Recovery = 89% Analysis Date = 05/28/15 Pct Recovery = 89% Analysis Date = 05/18/15 Pct Recovery = 89% Analysis Date = 05/18/15 Pct Recovery = 89% Analysis Date = 05/07/15 Pct Recovery = 89% Analysis Date = 05/07/15 Pct Recovery = 89% Analysis Date = 04/26/15 Pct Recovery = 89% Analysis Date = 04/26/15 Pct Recovery = 89% Analysis Date = 04/15/15 Pct Recovery = 89% Analysis Date = 04/15/15 Pct Recovery = 89% Analysis Date = 04/04/15 Pct Recovery = 88% Analysis Date = 04/04/15 Pct Recovery = 88% Analysis Date = 03/25/15 Pct Recovery = 88% Analysis Date = 03/25/15 Pct Recovery = 88% Analysis Date = 03/14/15 Pct Recovery = 88% Analysis Date = 03/14/15 Pct Recovery = 88% Analysis Date = 03/03/15 Pct Recovery = 88% Analysis Date = 03/03/15 Pct Recovery = 88% Analysis Date = 02/20/15 Pct Recovery = 87% Analysis Date = 02/20/15 Pct Recovery = 87% Analysis Date = 02/10/15 Pct Recovery = 87% Analysis Date = 02/10/15 Pct Recovery = 87% Analysis Date = 01/30/15 Pct Recovery = 87% Analysis Date = 01/30/15 Pct Recovery = 87% Analysis Date = 01/19/15 Pct Recovery = 87% Analysis Date = 01/19/15 Pct Recovery = 87% Analysis Date = 01/08/15 Pct Recovery = 86% Analysis Date = 01/08/15 Pct Recovery = 86% Analysis Date = 12/28/14 Pct Recovery = 86% Analysis Date = 12/28/14 Pct Recovery = 86% Analysis Date = 12/18/14 Pct Recovery = 86% Analysis Date = 12/18/14 Pct Recovery = 86% Analysis Date = 12/07/14 Pct Recovery = 86% Analysis Date = 12/07/14 Pct Recovery = 86% Analysis Date = 11/26/14 Pct Recovery = 85% Analysis Date = 11/26/14 Pct Recovery = 85% Analysis Date = 11/15/14 Pct Recovery = 85% Analysis Date = 11/15/14 Pct Recovery = 85% Analysis Date = 11/05/14 Pct Recovery = 85% Analysis Date = 11/05/14 Pct Recovery = 85% Analysis Date = 10/25/14 Pct Recovery = 84% Analysis Date = 10/25/14 Pct Recovery = 84% Analysis Date = 10/14/14 Pct Recovery = 84% Analysis Date = 10/14/14 Pct Recovery = 84% Analysis Date = 10/03/14 Pct Recovery = 84% Analysis Date = 10/03/14 Pct Recovery = 84% Analysis Date = 09/23/14 Pct Recovery = 84% Analysis Date = 09/23/14 Pct Recovery = 84% Analysis Date = 09/12/14 Pct Recovery = 83% Analysis Date = 09/12/14 Pct Recovery = 83% Analysis Date = 09/01/14 Pct Recovery = 83% Analysis Date = 09/01/14 Pct Recovery = 83% Analysis Date = 08/21/14 Pct Recovery = 83% Analysis Date = 08/21/14 Pct Recovery = 83% Analysis Date = 08/10/14 Pct Recovery = 82% Analysis Date = 08/10/14 Pct Recovery = 82% Analysis Date = 07/31/14 Pct Recovery = 82% Analysis Date = 07/31/14 Pct Recovery = 82% Analysis Date = 07/20/14 Pct Recovery = 82% Analysis Date = 07/20/14 Pct Recovery = 82% Analysis Date = 07/09/14 Pct Recovery = 82% Analysis Date = 07/09/14 Pct Recovery = 82% Analysis Date = 06/28/14 Pct Recovery = 81% Analysis Date = 06/28/14 Pct Recovery = 81% Analysis Date = 06/18/14 Pct Recovery = 81% Analysis Date = 06/18/14 Pct Recovery = 81% Analysis Date = 06/07/14 Pct Recovery = 81% Analysis Date = 06/07/14 Pct Recovery = 81% Analysis Date = 05/27/14 Pct Recovery = 81% Analysis Date = 05/27/14 Pct Recovery = 81% Analysis Date = 05/16/14 Pct Recovery = 80% Analysis Date = 05/16/14 Pct Recovery = 80% Analysis Date = 05/05/14 Pct Recovery = 80% Analysis Date = 05/05/14 Pct Recovery = 80% Analysis Date = 04/25/14 Pct Recovery = 80% Analysis Date = 04/25/14 Pct Recovery = 80% Analysis Date = 04/14/14 Pct Recovery = 80% Analysis Date = 04/14/14 Pct Recovery = 80% Analysis Date = 04/03/14 Pct Recovery = 79% Analysis Date = 04/03/14 Pct Recovery = 79% Analysis Date = 03/23/14 Pct Recovery = 79% Analysis Date = 03/23/14 Pct Recovery = 79% Analysis Date = 03/13/14 Pct Recovery = 79% Analysis Date = 03/13/14 Pct Recovery = 79% Analysis Date = 03/02/14 Pct Recovery = 79% Analysis Date = 03/02/14 Pct Recovery = 79% Analysis Date = 02/19/14 Pct Recovery = 78% Analysis Date = 02/19/14 Pct Recovery = 78% Analysis Date = 02/08/14 Pct Recovery = 78% Analysis Date = 02/08/14 Pct Recovery = 78% Analysis Date = 01/28/14 Pct Recovery = 78% Analysis Date = 01/28/14 Pct Recovery = 78% Analysis Date = 01/18/14 Pct Recovery = 77% Analysis Date = 01/18/14 Pct Recovery = 77% Analysis Date = 01/07/14 Pct Recovery = 77% Analysis Date = 01/07/14 Pct Recovery = 77% Analysis Date = 12/27/13 Pct Recovery = 77% Analysis Date = 12/27/13 Pct Recovery = 77% Analysis Date = 12/16/13 Pct Recovery = 76% Analysis Date = 12/16/13 Pct Recovery = 76% Analysis Date = 12/06/13 Pct Recovery = 76% Analysis Date = 12/06/13 Pct Recovery = 76% Analysis Date = 11/25/13 Pct Recovery = 76% Analysis Date = 11/25/13 Pct Recovery = 76% Analysis Date = 11/14/13 Pct Recovery = 76% Analysis Date = 11/14/13 Pct Recovery = 76% Analysis Date = 11/03/13 Pct Recovery = 75% Analysis Date = 11/03/13 Pct Recovery = 75% Analysis Date = 10/23/13 Pct Recovery = 75% Analysis Date = 10/23/13 Pct Recovery = 75% Analysis Date = 10/13/13 Pct Recovery = 75% Analysis Date = 10/13/13 Pct Recovery = 75% Analysis Date = 10/02/13 Pct Recovery = 74% Analysis Date = 10/02/13 Pct Recovery = 74% Analysis Date = 09/21/13 Pct Recovery = 74% Analysis Date = 09/21/13 Pct Recovery = 74% Analysis Date = 09/10/13 Pct Recovery = 74% Analysis Date = 09/10/13 Pct Recovery = 74% Analysis Date = 08/31/13 Pct Recovery = 74% Analysis Date = 08/31/13 Pct Recovery = 74% Analysis Date = 08/20/13 Pct Recovery = 73% Analysis Date = 08/20/13 Pct Recovery = 73% Analysis Date = 08/09/13 Pct Recovery = 73% Analysis Date = 08/09/13 Pct Recovery = 73% Analysis Date = 07/29/13 Pct Recovery = 73% Analysis Date = 07/29/13 Pct Recovery = 73% Analysis Date = 07/19/13 Pct Recovery = 73% Analysis Date = 07/19/13 Pct Recovery = 73% Analysis Date = 07/08/13 Pct Recovery = 73% Analysis Date = 07/08/13 Pct Recovery = 73% Analysis Date = 06/27/13 Pct Recovery = 72% Analysis Date = 06/27/13 Pct Recovery = 72% Analysis Date = 06/16/13 Pct Recovery = 72% Analysis Date = 06/16/13 Pct Recovery = 72% Analysis Date = 06/05/13 Pct Recovery = 72% Analysis Date = 06/05/13 Pct Recovery = 72% Analysis Date = 05/26/13 Pct Recovery = 72% Analysis Date = 05/26/13 Pct Recovery = 72% Analysis Date = 05/15/13 Pct Recovery = 72% Analysis Date = 05/15/13 Pct Recovery = 72% Analysis Date = 05/04/13 Pct Recovery = 72% Analysis Date = 05/04/13 Pct Recovery = 72% Analysis Date = 04/23/13 Pct Recovery = 72% Analysis Date = 04/23/13 Pct Recovery = 72% Analysis Date = 04/13/13 Pct Recovery = 72% Analysis Date = 04/13/13 Pct Recovery = 72% Analysis Date = 04/02/13 Pct Recovery = 71% Analysis Date = 04/02/13 Pct Recovery = 71% Analysis Date = 03/22/13 Pct Recovery = 71% Analysis Date = 03/22/13 Pct Recovery = 71% Analysis Date = 03/11/13 Pct Recovery = 71% Analysis Date = 03/11/13 Pct Recovery = 71% Analysis Date = 02/28/13 Pct Recovery = 71% Analysis Date = 02/28/13 Pct Recovery = 71% Analysis Date = 02/18/13 Pct Recovery = 71% Analysis Date = 02/18/13 Pct Recovery = 71% Analysis Date = 02/07/13 Pct Recovery = 71% Analysis Date = 02/07/13 Pct Recovery = 71% Analysis Date = 01/27/13 Pct Recovery = 71% Analysis Date = 01/27/13 Pct Recovery = 71% Analysis Date = 01/16/13 Pct Recovery = 71% Analysis Date = 01/16/13 Pct Recovery = 71% Analysis Date = 01/06/13 Pct Recovery = 71% Analysis Date = 01/06/13 Pct Recovery = 71% Analysis Date = 12/26/12 Pct Recovery = 72% Analysis Date = 12/26/12 Pct Recovery = 72% Analysis Date = 12/15/12 Pct Recovery = 72% Analysis Date = 12/15/12 Pct Recovery = 72% Analysis Date = 12/04/12 Pct Recovery = 72% Analysis Date = 12/04/12 Pct Recovery = 72% Analysis Date = 11/23/12 Pct Recovery = 72% Analysis Date = 11/23/12 Pct Recovery = 72% Analysis Date = 11/13/12 Pct Recovery = 72% Analysis Date = 11/13/12 Pct Recovery = 72% Analysis Date = 11/02/12 Pct Recovery = 72% Analysis Date = 11/02/12 Pct Recovery = 72% Analysis Date = 10/22/12 Pct Recovery = 72% Analysis Date = 10/22/12 Pct Recovery = 72% Analysis Date = 10/11/12 Pct Recovery = 72% Analysis Date = 10/11/12 Pct Recovery = 72% Analysis Date = 10/01/12 Pct Recovery = 72% Analysis Date = 10/01/12 Pct Recovery = 72% Analysis Date = 09/20/12 Pct Recovery = 72% Analysis Date = 09/20/12 Pct Recovery = 72% Analysis Date = 09/09/12 Pct Recovery = 72% Analysis Date = 09/09/12 Pct Recovery = 72% Analysis Date = 08/29/12 Pct Recovery = 73% Analysis Date = 08/29/12 Pct Recovery = 73% Analysis Date = 08/18/12 Pct Recovery = 73% Analysis Date = 08/18/12 Pct Recovery = 73% Analysis Date = 08/08/12 Pct Recovery = 73% Analysis Date = 08/08/12 Pct Recovery = 73% Analysis Date = 07/28/12 Pct Recovery = 73% Analysis Date = 07/28/12 Pct Recovery = 73% Analysis Date = 07/17/12 Pct Recovery = 73% Analysis Date = 07/17/12 Pct Recovery = 73% Analysis Date = 07/06/12 Pct Recovery = 73% Analysis Date = 07/06/12 Pct Recovery = 73% Analysis Date = 06/26/12 Pct Recovery = 73% Analysis Date = 06/26/12 Pct Recovery = 73% Analysis Date = 06/15/12 Pct Recovery = 73% Analysis Date = 06/15/12 Pct Recovery = 73% Analysis Date = 06/04/12 Pct Recovery = 73% Analysis Date = 06/04/12 Pct Recovery = 73% Analysis Date = 05/24/12 Pct Recovery = 73% Analysis Date = 05/24/12 Pct Recovery = 73% Analysis Date = 05/14/12 Pct Recovery = 73% Analysis Date = 05/14/12 Pct Recovery = 73% Analysis Date = 05/03/12 Pct Recovery = 73% Analysis Date = 05/03/12 Pct Recovery = 73% Analysis Date = 04/22/12 Pct Recovery = 73% Analysis Date = 04/22/12 Pct Recovery = 73% Analysis Date = 04/11/12 Pct Recovery = 73% Analysis Date = 04/11/12 Pct Recovery = 73% Analysis Date = 03/31/12 Pct Recovery = 73% Analysis Date = 03/31/12 Pct Recovery = 73% Analysis Date = 03/21/12 Pct Recovery = 73% Analysis Date = 03/21/12 Pct Recovery = 73% Analysis Date = 03/10/12 Pct Recovery = 73% Analysis Date = 03/10/12 Pct Recovery = 73% Analysis Date = 02/28/12 Pct Recovery = 73% Analysis Date = 02/28/12 Pct Recovery = 73% Analysis Date = 02/17/12 Pct Recovery = 73% Analysis Date = 02/17/12 Pct Recovery = 73% Analysis Date = 02/07/12 Pct Recovery = 73% Analysis Date = 02/07/12 Pct Recovery = 73% Analysis Date = 01/27/12 Pct Recovery = 73% Analysis Date = 01/27/12 Pct Recovery = 73% Analysis Date = 01/16/12 Pct Recovery = 73% Analysis Date = 01/16/12 Pct Recovery = 73% Analysis Date = 01/05/12 Pct Recovery = 73% Analysis Date = 01/05/12 Pct Recovery = 73% Analysis Date = 12/25/11 Pct Recovery = 73% Analysis Date = 12/25/11 Pct Recovery = 73% Analysis Date = 12/15/11 Pct Recovery = 73% Analysis Date = 12/15/11 Pct Recovery = 73% Analysis Date = 12/04/11 Pct Recovery = 73% Analysis Date = 12/04/11 Pct Recovery = 73% Analysis Date = 11/23/11 Pct Recovery = 73% Analysis Date = 11/23/11 Pct Recovery = 73% Analysis Date = 11/12/11 Pct Recovery = 73% Analysis Date = 11/12/11 Pct Recovery = 73% Analysis Date = 11/02/11 Pct Recovery = 73% Analysis Date = 11/02/11 Pct Recovery = 73% Analysis Date = 10/22/11 Pct Recovery = 73% Analysis Date = 10/22/11 Pct Recovery = 73% Analysis Date = 10/11/11 Pct Recovery = 73% Analysis Date = 10/11/11 Pct Recovery = 73% Analysis Date = 09/30/11 Pct Recovery = 73% Analysis Date = 09/30/11 Pct Recovery = 73% Analysis Date = 09/19/11 Pct Recovery = 73% Analysis Date = 09/19/11 Pct Recovery = 73% Analysis Date = 09/09/11 Pct Recovery = 73% Analysis Date = 09/09/11 Pct Recovery = 73% Analysis Date = 08/29/11 Pct Recovery = 73% Analysis Date = 08/29/11 Pct Recovery = 73% Analysis Date = 08/18/11 Pct Recovery = 73% Analysis Date = 08/18/11 Pct Recovery = 73% Analysis Date = 08/07/11 Pct Recovery = 73% Analysis Date = 08/07/11 Pct Recovery = 73% Analysis Date = 07/28/11 Pct Recovery = 73% Analysis Date = 07/28/11 Pct Recovery = 73% Analysis Date = 07/17/11 Pct Recovery = 73% Analysis Date = 07/17/11 Pct Recovery = 73% Analysis Date = 07/06/11 Pct Recovery = 73% Analysis Date = 07/06/11 Pct Recovery = 73% Analysis Date = 06/25/11 Pct Recovery = 73% Analysis Date = 06/25/11 Pct Recovery = 73% Analysis Date = 06/14/11 Pct Recovery = 73% Analysis Date = 06/14/11 Pct Recovery = 73% Analysis Date = 06/04/11 Pct Recovery = 73% Analysis Date = 06/04/11 Pct Recovery = 73% Analysis Date = 05/24/11 Pct Recovery = 73% Analysis Date = 05/24/11 Pct Recovery = 73% Analysis Date = 05/13/11 Pct Recovery = 73% Analysis Date = 05/13/11 Pct Recovery = 73% Analysis Date = 05/02/11 Pct Recovery = 73% Analysis Date = 05/02/11 Pct Recovery = 73% Analysis Date = 04/22/11 Pct Recovery = 72% Analysis Date = 04/22/11 Pct Recovery = 72% Analysis Date = 04/11/11 Pct Recovery = 72% Analysis Date = 04/11/11 Pct Recovery = 72% Analysis Date = 03/31/11 Pct Recovery = 72% Analysis Date = 03/31/11 Pct Recovery = 72% Analysis Date = 03/20/11 Pct Recovery = 72% Analysis Date = 03/20/11 Pct Recovery = 72% Analysis Date = 03/10/11 Pct Recovery = 72% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
NORETHINDRONE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 58 79% 18% 75% 16%
Total 58 79% 18% 75% 16%

Sample Statistics
NORETHINDRONE

Characteristic N % % Basis
Plotted 58 73% Spiked
Estimated Values 1 1% Spiked
Deleted Values 2 2% Spiked + Not Spiked
Spiked, Censored 3 4% Spiked
Spiked 80 .  
False Negatives 18 23% 18 out of 79
Not Spiked 51 .  
False Positives 0 0% 0 out of 50

BQS OBSP Determination:
PROGESTERONE
METHOD: 4434 , TESTIDCODE: 64543GM005
Open Data Set

Analysis Date = 02/01/12 SpikeMix = Spex Organics T1100629008: 100 µl Pct Recovery = 36% Analysis Date = 09/29/11 SpikeMix = Spex Organics T1100629008: 100 µl Pct Recovery = 60% Analysis Date = 03/31/11 SpikeMix = Spex Organics T1100629008: 100 µl Pct Recovery = 42% Analysis Date = 05/09/11 SpikeMix = Abs 081810: 100 µl Pct Recovery = 50% Analysis Date = 07/02/12 SpikeMix = Abs 081810: 100 µl Pct Recovery = 93% Analysis Date = 04/17/12 SpikeMix = Abs 081810: 100 µl Pct Recovery = 85% Analysis Date = 10/03/11 SpikeMix = Abs 081810: 100 µl Pct Recovery = 51% Analysis Date = 08/31/16 SpikeMix = Spex Organics TS160420010: 50 µl & ChemService 5016200: 50 µl Pct Recovery = 57% Analysis Date = 12/15/16 SpikeMix = Abs 061416H: 50 µl & ChemService 5016100: 50 µl Pct Recovery = 40% Analysis Date = 04/01/15 SpikeMix = ERA 0227-14-07.2: 60 µl & ChemService 2561700: 60 µl Pct Recovery = 31% Analysis Date = 08/22/14 SpikeMix = ERA 0227-14-07.2: 60 µl & Abs 042114: 60 µl Pct Recovery = 27% Analysis Date = 08/11/14 SpikeMix = Abs 031014: 60 µl & ERA 0227-14-07.2: 60 µl Pct Recovery = 34% Analysis Date = 04/01/15 SpikeMix = Spex Organics E1140505004: 60 µl & Supelco LC06946: 60 µl Pct Recovery = 19% Analysis Date = 02/12/15 SpikeMix = Supelco LC06946: 60 µl & Abs 042114: 60 µl Pct Recovery = 27% Analysis Date = 12/09/14 SpikeMix = Abs 031014: 60 µl & Supelco LC06946: 60 µl Pct Recovery = 24% Analysis Date = 09/23/14 SpikeMix = Supelco LC06946: 60 µl & ChemService 2561700: 60 µl Pct Recovery = 51% Analysis Date = 03/14/14 SpikeMix = Supelco LB99393: 50 µl & Abs 050813: 50 µl Pct Recovery = 28% Analysis Date = 02/25/14 SpikeMix = ERA 0415-13-01.1A: 50 µl & Abs 050813: 50 µl Pct Recovery = 28% Analysis Date = 03/14/14 SpikeMix = ERA 0415-13-01.2A: 50 µl & Spex Organics T1130423008: 50 µl Pct Recovery = 36% Analysis Date = 03/05/14 SpikeMix = Spex Organics T1130423008: 50 µl & Abs 071513: 50 µl Pct Recovery = 41% Analysis Date = 08/09/13 SpikeMix = ERA 0415-13-01.2A: 50 µl & Spex Organics T1130423008: 50 µl Pct Recovery = 37% Analysis Date = 12/03/12 SpikeMix = ERA 0511-12-02: 50 µl & Abs 051512: 50 µl Pct Recovery = 41% Analysis Date = 01/08/16 SpikeMix = Spex Organics EN150501025: 60 µl & ERA 0601-15-04: 60 µl Pct Recovery = 47% Analysis Date = 01/05/16 SpikeMix = Supelco LC13547: 60 µl & ChemService 4073900: 60 µl Pct Recovery = 47% Analysis Date = 02/22/13 SpikeMix = Restek A089631: 50 µl & Supelco LB92781: 50 µl Pct Recovery = 49% Analysis Date = 12/18/12 SpikeMix = Spex Organics T1120525010: 50 µl & Supelco LB92781: 50 µl Pct Recovery = 44% Analysis Date = 01/13/17 SpikeMix = Abs 052616: 30 µl & ChemService 5016200: 30 µl Pct Recovery = 47% Analysis Date = 09/21/16 SpikeMix = ChemService 5016200: 30 µl & ChemService 5016100: 30 µl Pct Recovery = 36% Analysis Date = 09/16/16 SpikeMix = Spex Organics EN160621015: 30 µl & ChemService 5016200: 30 µl Pct Recovery = 44% Analysis Date = 12/05/16 SpikeMix = Abs 052616: 30 µl & Abs 061416H: 30 µl Pct Recovery = 42% Analysis Date = 07/12/16 SpikeMix = Spex Organics EN150501025: 50 µl & ERA 0601-15-04: 50 µl Pct Recovery = 36% Analysis Date = 06/24/16 SpikeMix = ERA 0601-15-04: 50 µl & ChemService 4073900: 50 µl Pct Recovery = 34% Analysis Date = 03/07/16 SpikeMix = Abs 041515: 50 µl & ERA 0601-15-04: 50 µl Pct Recovery = 62% Analysis Date = 12/10/15 SpikeMix = Abs 041515: 50 µl & ERA 0601-15-04: 50 µl Pct Recovery = 64% Analysis Date = 09/14/15 SpikeMix = ERA 0601-15-04: 50 µl & ChemService 4073900: 50 µl Pct Recovery = 42% Analysis Date = 08/10/15 SpikeMix = ERA 0601-15-04: 50 µl & Crescent 04EE007: 50 µl Pct Recovery = 32% Analysis Date = 11/05/14 SpikeMix = ERA 0227-14-07.2: 30 µl & Abs 042114: 30 µl Pct Recovery = 49% Analysis Date = 09/04/14 SpikeMix = ERA 0227-14-07.2: 30 µl & Spex Organics E1140505004: 30 µl Pct Recovery = 51% Analysis Date = 07/28/14 SpikeMix = ERA 0227-14-07.2: 30 µl & ChemService 2561700: 30 µl Pct Recovery = 67% Analysis Date = 07/14/14 SpikeMix = ERA 0227-14-07.2: 30 µl & Abs 031014: 30 µl Pct Recovery = 61% Analysis Date = 01/29/15 SpikeMix = Abs 031014: 30 µl & Supelco LC06946: 30 µl Pct Recovery = 32% Analysis Date = 01/21/15 SpikeMix = Supelco LC06946: 30 µl & ChemService 2561700: 30 µl Pct Recovery = 34% Analysis Date = 12/23/14 SpikeMix = Spex Organics E1140505004: 30 µl & Supelco LC06946: 30 µl Pct Recovery = 35% Analysis Date = 12/16/14 SpikeMix = Supelco LC06946: 30 µl & Abs 042114: 30 µl Pct Recovery = 32% Analysis Date = 04/03/13 SpikeMix = Spex Organics T1120525010: 25 µl & Abs 051512: 25 µl Pct Recovery = 42% Analysis Date = 11/01/12 SpikeMix = ERA 0507-12-04.1: 25 µl & Abs 051512: 25 µl Pct Recovery = 67% Analysis Date = 08/31/12 SpikeMix = ERA 0511-12-02: 25 µl & Abs 051512: 25 µl Pct Recovery = 51% Analysis Date = 08/24/12 SpikeMix = Abs 051512: 25 µl Pct Recovery = 48% Analysis Date = 01/08/16 SpikeMix = ERA 0601-15-04: 30 µl & ChemService 4073900: 30 µl Pct Recovery = 36% Analysis Date = 11/02/15 SpikeMix = Supelco LC13547: 30 µl & Crescent 04EE007: 30 µl Pct Recovery = 39% Analysis Date = 03/03/14 SpikeMix = Abs 050813: 20 µl & Abs 071513: 20 µl Pct Recovery = 31% Analysis Date = 02/19/14 SpikeMix = Abs 050813: 20 µl & Abs 071513: 20 µl Pct Recovery = 27% Analysis Date = 11/18/13 SpikeMix = ERA 0415-13-01.2A: 20 µl & Abs 050813: 20 µl Pct Recovery = 38% Analysis Date = 12/09/13 SpikeMix = Supelco LB99393: 20 µl & Spex Organics T1130423008: 20 µl Pct Recovery = 30% Analysis Date = 06/27/13 SpikeMix = ERA 0415-13-01.1A: 20 µl & Spex Organics T1130423008: 20 µl Pct Recovery = 23% Analysis Date = 06/04/13 SpikeMix = Supelco LB99393: 20 µl & Spex Organics T1130423008: 20 µl Pct Recovery = 45% Analysis Date = 05/26/11 SpikeMix = Spex Organics T1100629008: 25 µl Pct Recovery = 44% Analysis Date = 04/10/13 SpikeMix = ERA 0511-12-02: 25 µl & Supelco LB92781: 25 µl Pct Recovery = 73% Analysis Date = 02/08/13 SpikeMix = ERA 0507-12-04.1: 25 µl & Supelco LB92781: 25 µl Pct Recovery = 48% Analysis Date = 12/18/12 SpikeMix = Restek A089631: 25 µl & Supelco LB92781: 25 µl Pct Recovery = 38% Analysis Date = 08/16/12 SpikeMix = Spex Organics T1100629008: 25 µl Pct Recovery = 61% Analysis Date = 11/28/11 SpikeMix = Spex Organics T1100629008: 25 µl Pct Recovery = 35% Analysis Date = 10/13/11 SpikeMix = Spex Organics T1100629008: 25 µl Pct Recovery = 32% Analysis Date = 03/10/11 SpikeMix = Spex Organics T1100629008: 25 µl Pct Recovery = 58% Analysis Date = 07/11/11 SpikeMix = Spex Organics T1100629008: 25 µl Pct Recovery = 51% Analysis Date = 03/27/12 SpikeMix = Abs 081810: 25 µl Pct Recovery = 71% Analysis Date = 10/12/11 SpikeMix = Abs 081810: 25 µl Pct Recovery = 42% Analysis Date = 06/13/11 SpikeMix = Abs 081810: 25 µl Pct Recovery = 58% Analysis Date = 03/30/11 SpikeMix = Abs 081810: 25 µl Pct Recovery = 77% Analysis Date = 01/13/17 Pct Recovery = 45% Analysis Date = 01/02/17 Pct Recovery = 45% Analysis Date = 01/02/17 Pct Recovery = 45% Analysis Date = 12/22/16 Pct Recovery = 45% Analysis Date = 12/22/16 Pct Recovery = 45% Analysis Date = 12/11/16 Pct Recovery = 45% Analysis Date = 12/11/16 Pct Recovery = 45% Analysis Date = 12/01/16 Pct Recovery = 45% Analysis Date = 12/01/16 Pct Recovery = 45% Analysis Date = 11/20/16 Pct Recovery = 45% Analysis Date = 11/20/16 Pct Recovery = 45% Analysis Date = 11/09/16 Pct Recovery = 44% Analysis Date = 11/09/16 Pct Recovery = 44% Analysis Date = 10/30/16 Pct Recovery = 44% Analysis Date = 10/30/16 Pct Recovery = 44% Analysis Date = 10/19/16 Pct Recovery = 44% Analysis Date = 10/19/16 Pct Recovery = 44% Analysis Date = 10/08/16 Pct Recovery = 44% Analysis Date = 10/08/16 Pct Recovery = 44% Analysis Date = 09/28/16 Pct Recovery = 44% Analysis Date = 09/28/16 Pct Recovery = 44% Analysis Date = 09/17/16 Pct Recovery = 44% Analysis Date = 09/17/16 Pct Recovery = 44% Analysis Date = 09/06/16 Pct Recovery = 44% Analysis Date = 09/06/16 Pct Recovery = 44% Analysis Date = 08/27/16 Pct Recovery = 44% Analysis Date = 08/27/16 Pct Recovery = 44% Analysis Date = 08/16/16 Pct Recovery = 44% Analysis Date = 08/16/16 Pct Recovery = 44% Analysis Date = 08/05/16 Pct Recovery = 44% Analysis Date = 08/05/16 Pct Recovery = 44% Analysis Date = 07/26/16 Pct Recovery = 43% Analysis Date = 07/26/16 Pct Recovery = 43% Analysis Date = 07/15/16 Pct Recovery = 43% Analysis Date = 07/15/16 Pct Recovery = 43% Analysis Date = 07/04/16 Pct Recovery = 43% Analysis Date = 07/04/16 Pct Recovery = 43% Analysis Date = 06/24/16 Pct Recovery = 43% Analysis Date = 06/24/16 Pct Recovery = 43% Analysis Date = 06/13/16 Pct Recovery = 43% Analysis Date = 06/13/16 Pct Recovery = 43% Analysis Date = 06/02/16 Pct Recovery = 43% Analysis Date = 06/02/16 Pct Recovery = 43% Analysis Date = 05/23/16 Pct Recovery = 43% Analysis Date = 05/23/16 Pct Recovery = 43% Analysis Date = 05/12/16 Pct Recovery = 43% Analysis Date = 05/12/16 Pct Recovery = 43% Analysis Date = 05/01/16 Pct Recovery = 43% Analysis Date = 05/01/16 Pct Recovery = 43% Analysis Date = 04/21/16 Pct Recovery = 42% Analysis Date = 04/21/16 Pct Recovery = 42% Analysis Date = 04/10/16 Pct Recovery = 42% Analysis Date = 04/10/16 Pct Recovery = 42% Analysis Date = 03/30/16 Pct Recovery = 42% Analysis Date = 03/30/16 Pct Recovery = 42% Analysis Date = 03/19/16 Pct Recovery = 42% Analysis Date = 03/19/16 Pct Recovery = 42% Analysis Date = 03/09/16 Pct Recovery = 42% Analysis Date = 03/09/16 Pct Recovery = 42% Analysis Date = 02/27/16 Pct Recovery = 42% Analysis Date = 02/27/16 Pct Recovery = 42% Analysis Date = 02/16/16 Pct Recovery = 42% Analysis Date = 02/16/16 Pct Recovery = 42% Analysis Date = 02/06/16 Pct Recovery = 42% Analysis Date = 02/06/16 Pct Recovery = 42% Analysis Date = 01/26/16 Pct Recovery = 42% Analysis Date = 01/26/16 Pct Recovery = 42% Analysis Date = 01/15/16 Pct Recovery = 42% Analysis Date = 01/15/16 Pct Recovery = 42% Analysis Date = 01/05/16 Pct Recovery = 42% Analysis Date = 01/05/16 Pct Recovery = 42% Analysis Date = 12/25/15 Pct Recovery = 41% Analysis Date = 12/25/15 Pct Recovery = 41% Analysis Date = 12/14/15 Pct Recovery = 41% Analysis Date = 12/14/15 Pct Recovery = 41% Analysis Date = 12/04/15 Pct Recovery = 41% Analysis Date = 12/04/15 Pct Recovery = 41% Analysis Date = 11/23/15 Pct Recovery = 41% Analysis Date = 11/23/15 Pct Recovery = 41% Analysis Date = 11/12/15 Pct Recovery = 41% Analysis Date = 11/12/15 Pct Recovery = 41% Analysis Date = 11/02/15 Pct Recovery = 41% Analysis Date = 11/02/15 Pct Recovery = 41% Analysis Date = 10/22/15 Pct Recovery = 41% Analysis Date = 10/22/15 Pct Recovery = 41% Analysis Date = 10/11/15 Pct Recovery = 41% Analysis Date = 10/11/15 Pct Recovery = 41% Analysis Date = 10/01/15 Pct Recovery = 41% Analysis Date = 10/01/15 Pct Recovery = 41% Analysis Date = 09/20/15 Pct Recovery = 41% Analysis Date = 09/20/15 Pct Recovery = 41% Analysis Date = 09/09/15 Pct Recovery = 41% Analysis Date = 09/09/15 Pct Recovery = 41% Analysis Date = 08/30/15 Pct Recovery = 41% Analysis Date = 08/30/15 Pct Recovery = 41% Analysis Date = 08/19/15 Pct Recovery = 40% Analysis Date = 08/19/15 Pct Recovery = 40% Analysis Date = 08/08/15 Pct Recovery = 40% Analysis Date = 08/08/15 Pct Recovery = 40% Analysis Date = 07/29/15 Pct Recovery = 40% Analysis Date = 07/29/15 Pct Recovery = 40% Analysis Date = 07/18/15 Pct Recovery = 40% Analysis Date = 07/18/15 Pct Recovery = 40% Analysis Date = 07/07/15 Pct Recovery = 40% Analysis Date = 07/07/15 Pct Recovery = 40% Analysis Date = 06/26/15 Pct Recovery = 40% Analysis Date = 06/26/15 Pct Recovery = 40% Analysis Date = 06/16/15 Pct Recovery = 40% Analysis Date = 06/16/15 Pct Recovery = 40% Analysis Date = 06/05/15 Pct Recovery = 40% Analysis Date = 06/05/15 Pct Recovery = 40% Analysis Date = 05/25/15 Pct Recovery = 40% Analysis Date = 05/25/15 Pct Recovery = 40% Analysis Date = 05/15/15 Pct Recovery = 40% Analysis Date = 05/15/15 Pct Recovery = 40% Analysis Date = 05/04/15 Pct Recovery = 40% Analysis Date = 05/04/15 Pct Recovery = 40% Analysis Date = 04/23/15 Pct Recovery = 40% Analysis Date = 04/23/15 Pct Recovery = 40% Analysis Date = 04/13/15 Pct Recovery = 39% Analysis Date = 04/13/15 Pct Recovery = 39% Analysis Date = 04/02/15 Pct Recovery = 39% Analysis Date = 04/02/15 Pct Recovery = 39% Analysis Date = 03/22/15 Pct Recovery = 39% Analysis Date = 03/22/15 Pct Recovery = 39% Analysis Date = 03/12/15 Pct Recovery = 39% Analysis Date = 03/12/15 Pct Recovery = 39% Analysis Date = 03/01/15 Pct Recovery = 39% Analysis Date = 03/01/15 Pct Recovery = 39% Analysis Date = 02/18/15 Pct Recovery = 39% Analysis Date = 02/18/15 Pct Recovery = 39% Analysis Date = 02/08/15 Pct Recovery = 39% Analysis Date = 02/08/15 Pct Recovery = 39% Analysis Date = 01/28/15 Pct Recovery = 39% Analysis Date = 01/28/15 Pct Recovery = 39% Analysis Date = 01/17/15 Pct Recovery = 39% Analysis Date = 01/17/15 Pct Recovery = 39% Analysis Date = 01/07/15 Pct Recovery = 38% Analysis Date = 01/07/15 Pct Recovery = 38% Analysis Date = 12/27/14 Pct Recovery = 38% Analysis Date = 12/27/14 Pct Recovery = 38% Analysis Date = 12/16/14 Pct Recovery = 38% Analysis Date = 12/16/14 Pct Recovery = 38% Analysis Date = 12/06/14 Pct Recovery = 38% Analysis Date = 12/06/14 Pct Recovery = 38% Analysis Date = 11/25/14 Pct Recovery = 38% Analysis Date = 11/25/14 Pct Recovery = 38% Analysis Date = 11/14/14 Pct Recovery = 38% Analysis Date = 11/14/14 Pct Recovery = 38% Analysis Date = 11/04/14 Pct Recovery = 38% Analysis Date = 11/04/14 Pct Recovery = 38% Analysis Date = 10/24/14 Pct Recovery = 38% Analysis Date = 10/24/14 Pct Recovery = 38% Analysis Date = 10/13/14 Pct Recovery = 37% Analysis Date = 10/13/14 Pct Recovery = 37% Analysis Date = 10/02/14 Pct Recovery = 37% Analysis Date = 10/02/14 Pct Recovery = 37% Analysis Date = 09/22/14 Pct Recovery = 37% Analysis Date = 09/22/14 Pct Recovery = 37% Analysis Date = 09/11/14 Pct Recovery = 37% Analysis Date = 09/11/14 Pct Recovery = 37% Analysis Date = 08/31/14 Pct Recovery = 37% Analysis Date = 08/31/14 Pct Recovery = 37% Analysis Date = 08/21/14 Pct Recovery = 37% Analysis Date = 08/21/14 Pct Recovery = 37% Analysis Date = 08/10/14 Pct Recovery = 37% Analysis Date = 08/10/14 Pct Recovery = 37% Analysis Date = 07/30/14 Pct Recovery = 37% Analysis Date = 07/30/14 Pct Recovery = 37% Analysis Date = 07/20/14 Pct Recovery = 37% Analysis Date = 07/20/14 Pct Recovery = 37% Analysis Date = 07/09/14 Pct Recovery = 37% Analysis Date = 07/09/14 Pct Recovery = 37% Analysis Date = 06/28/14 Pct Recovery = 37% Analysis Date = 06/28/14 Pct Recovery = 37% Analysis Date = 06/18/14 Pct Recovery = 37% Analysis Date = 06/18/14 Pct Recovery = 37% Analysis Date = 06/07/14 Pct Recovery = 38% Analysis Date = 06/07/14 Pct Recovery = 38% Analysis Date = 05/27/14 Pct Recovery = 38% Analysis Date = 05/27/14 Pct Recovery = 38% Analysis Date = 05/17/14 Pct Recovery = 38% Analysis Date = 05/17/14 Pct Recovery = 38% Analysis Date = 05/06/14 Pct Recovery = 38% Analysis Date = 05/06/14 Pct Recovery = 38% Analysis Date = 04/25/14 Pct Recovery = 38% Analysis Date = 04/25/14 Pct Recovery = 38% Analysis Date = 04/15/14 Pct Recovery = 38% Analysis Date = 04/15/14 Pct Recovery = 38% Analysis Date = 04/04/14 Pct Recovery = 39% Analysis Date = 04/04/14 Pct Recovery = 39% Analysis Date = 03/24/14 Pct Recovery = 39% Analysis Date = 03/24/14 Pct Recovery = 39% Analysis Date = 03/14/14 Pct Recovery = 39% Analysis Date = 03/14/14 Pct Recovery = 39% Analysis Date = 03/03/14 Pct Recovery = 39% Analysis Date = 03/03/14 Pct Recovery = 39% Analysis Date = 02/20/14 Pct Recovery = 39% Analysis Date = 02/20/14 Pct Recovery = 39% Analysis Date = 02/10/14 Pct Recovery = 40% Analysis Date = 02/10/14 Pct Recovery = 40% Analysis Date = 01/30/14 Pct Recovery = 40% Analysis Date = 01/30/14 Pct Recovery = 40% Analysis Date = 01/19/14 Pct Recovery = 40% Analysis Date = 01/19/14 Pct Recovery = 40% Analysis Date = 01/08/14 Pct Recovery = 40% Analysis Date = 01/08/14 Pct Recovery = 40% Analysis Date = 12/29/13 Pct Recovery = 41% Analysis Date = 12/29/13 Pct Recovery = 41% Analysis Date = 12/18/13 Pct Recovery = 41% Analysis Date = 12/18/13 Pct Recovery = 41% Analysis Date = 12/07/13 Pct Recovery = 41% Analysis Date = 12/07/13 Pct Recovery = 41% Analysis Date = 11/27/13 Pct Recovery = 41% Analysis Date = 11/27/13 Pct Recovery = 41% Analysis Date = 11/16/13 Pct Recovery = 42% Analysis Date = 11/16/13 Pct Recovery = 42% Analysis Date = 11/05/13 Pct Recovery = 42% Analysis Date = 11/05/13 Pct Recovery = 42% Analysis Date = 10/26/13 Pct Recovery = 42% Analysis Date = 10/26/13 Pct Recovery = 42% Analysis Date = 10/15/13 Pct Recovery = 42% Analysis Date = 10/15/13 Pct Recovery = 42% Analysis Date = 10/04/13 Pct Recovery = 43% Analysis Date = 10/04/13 Pct Recovery = 43% Analysis Date = 09/24/13 Pct Recovery = 43% Analysis Date = 09/24/13 Pct Recovery = 43% Analysis Date = 09/13/13 Pct Recovery = 43% Analysis Date = 09/13/13 Pct Recovery = 43% Analysis Date = 09/02/13 Pct Recovery = 43% Analysis Date = 09/02/13 Pct Recovery = 43% Analysis Date = 08/23/13 Pct Recovery = 44% Analysis Date = 08/23/13 Pct Recovery = 44% Analysis Date = 08/12/13 Pct Recovery = 44% Analysis Date = 08/12/13 Pct Recovery = 44% Analysis Date = 08/01/13 Pct Recovery = 44% Analysis Date = 08/01/13 Pct Recovery = 44% Analysis Date = 07/22/13 Pct Recovery = 45% Analysis Date = 07/22/13 Pct Recovery = 45% Analysis Date = 07/11/13 Pct Recovery = 45% Analysis Date = 07/11/13 Pct Recovery = 45% Analysis Date = 06/30/13 Pct Recovery = 45% Analysis Date = 06/30/13 Pct Recovery = 45% Analysis Date = 06/20/13 Pct Recovery = 45% Analysis Date = 06/20/13 Pct Recovery = 45% Analysis Date = 06/09/13 Pct Recovery = 46% Analysis Date = 06/09/13 Pct Recovery = 46% Analysis Date = 05/29/13 Pct Recovery = 46% Analysis Date = 05/29/13 Pct Recovery = 46% Analysis Date = 05/19/13 Pct Recovery = 46% Analysis Date = 05/19/13 Pct Recovery = 46% Analysis Date = 05/08/13 Pct Recovery = 46% Analysis Date = 05/08/13 Pct Recovery = 46% Analysis Date = 04/27/13 Pct Recovery = 47% Analysis Date = 04/27/13 Pct Recovery = 47% Analysis Date = 04/16/13 Pct Recovery = 47% Analysis Date = 04/16/13 Pct Recovery = 47% Analysis Date = 04/06/13 Pct Recovery = 47% Analysis Date = 04/06/13 Pct Recovery = 47% Analysis Date = 03/26/13 Pct Recovery = 47% Analysis Date = 03/26/13 Pct Recovery = 47% Analysis Date = 03/15/13 Pct Recovery = 48% Analysis Date = 03/15/13 Pct Recovery = 48% Analysis Date = 03/05/13 Pct Recovery = 48% Analysis Date = 03/05/13 Pct Recovery = 48% Analysis Date = 02/22/13 Pct Recovery = 48% Analysis Date = 02/22/13 Pct Recovery = 48% Analysis Date = 02/11/13 Pct Recovery = 48% Analysis Date = 02/11/13 Pct Recovery = 48% Analysis Date = 02/01/13 Pct Recovery = 49% Analysis Date = 02/01/13 Pct Recovery = 49% Analysis Date = 01/21/13 Pct Recovery = 49% Analysis Date = 01/21/13 Pct Recovery = 49% Analysis Date = 01/10/13 Pct Recovery = 49% Analysis Date = 01/10/13 Pct Recovery = 49% Analysis Date = 12/31/12 Pct Recovery = 49% Analysis Date = 12/31/12 Pct Recovery = 49% Analysis Date = 12/20/12 Pct Recovery = 50% Analysis Date = 12/20/12 Pct Recovery = 50% Analysis Date = 12/09/12 Pct Recovery = 50% Analysis Date = 12/09/12 Pct Recovery = 50% Analysis Date = 11/29/12 Pct Recovery = 50% Analysis Date = 11/29/12 Pct Recovery = 50% Analysis Date = 11/18/12 Pct Recovery = 50% Analysis Date = 11/18/12 Pct Recovery = 50% Analysis Date = 11/07/12 Pct Recovery = 50% Analysis Date = 11/07/12 Pct Recovery = 50% Analysis Date = 10/28/12 Pct Recovery = 50% Analysis Date = 10/28/12 Pct Recovery = 50% Analysis Date = 10/17/12 Pct Recovery = 50% Analysis Date = 10/17/12 Pct Recovery = 50% Analysis Date = 10/06/12 Pct Recovery = 50% Analysis Date = 10/06/12 Pct Recovery = 50% Analysis Date = 09/26/12 Pct Recovery = 50% Analysis Date = 09/26/12 Pct Recovery = 50% Analysis Date = 09/15/12 Pct Recovery = 50% Analysis Date = 09/15/12 Pct Recovery = 50% Analysis Date = 09/04/12 Pct Recovery = 50% Analysis Date = 09/04/12 Pct Recovery = 50% Analysis Date = 08/25/12 Pct Recovery = 51% Analysis Date = 08/25/12 Pct Recovery = 51% Analysis Date = 08/14/12 Pct Recovery = 51% Analysis Date = 08/14/12 Pct Recovery = 51% Analysis Date = 08/03/12 Pct Recovery = 51% Analysis Date = 08/03/12 Pct Recovery = 51% Analysis Date = 07/23/12 Pct Recovery = 51% Analysis Date = 07/23/12 Pct Recovery = 51% Analysis Date = 07/13/12 Pct Recovery = 51% Analysis Date = 07/13/12 Pct Recovery = 51% Analysis Date = 07/02/12 Pct Recovery = 51% Analysis Date = 07/02/12 Pct Recovery = 51% Analysis Date = 06/21/12 Pct Recovery = 51% Analysis Date = 06/21/12 Pct Recovery = 51% Analysis Date = 06/11/12 Pct Recovery = 51% Analysis Date = 06/11/12 Pct Recovery = 51% Analysis Date = 05/31/12 Pct Recovery = 51% Analysis Date = 05/31/12 Pct Recovery = 51% Analysis Date = 05/20/12 Pct Recovery = 52% Analysis Date = 05/20/12 Pct Recovery = 52% Analysis Date = 05/10/12 Pct Recovery = 52% Analysis Date = 05/10/12 Pct Recovery = 52% Analysis Date = 04/29/12 Pct Recovery = 52% Analysis Date = 04/29/12 Pct Recovery = 52% Analysis Date = 04/18/12 Pct Recovery = 52% Analysis Date = 04/18/12 Pct Recovery = 52% Analysis Date = 04/08/12 Pct Recovery = 52% Analysis Date = 04/08/12 Pct Recovery = 52% Analysis Date = 03/28/12 Pct Recovery = 52% Analysis Date = 03/28/12 Pct Recovery = 52% Analysis Date = 03/17/12 Pct Recovery = 52% Analysis Date = 03/17/12 Pct Recovery = 52% Analysis Date = 03/07/12 Pct Recovery = 52% Analysis Date = 03/07/12 Pct Recovery = 52% Analysis Date = 02/25/12 Pct Recovery = 52% Analysis Date = 02/25/12 Pct Recovery = 52% Analysis Date = 02/14/12 Pct Recovery = 53% Analysis Date = 02/14/12 Pct Recovery = 53% Analysis Date = 02/04/12 Pct Recovery = 53% Analysis Date = 02/04/12 Pct Recovery = 53% Analysis Date = 01/24/12 Pct Recovery = 53% Analysis Date = 01/24/12 Pct Recovery = 53% Analysis Date = 01/13/12 Pct Recovery = 53% Analysis Date = 01/13/12 Pct Recovery = 53% Analysis Date = 01/03/12 Pct Recovery = 53% Analysis Date = 01/03/12 Pct Recovery = 53% Analysis Date = 12/23/11 Pct Recovery = 53% Analysis Date = 12/23/11 Pct Recovery = 53% Analysis Date = 12/12/11 Pct Recovery = 53% Analysis Date = 12/12/11 Pct Recovery = 53% Analysis Date = 12/02/11 Pct Recovery = 53% Analysis Date = 12/02/11 Pct Recovery = 53% Analysis Date = 11/21/11 Pct Recovery = 53% Analysis Date = 11/21/11 Pct Recovery = 53% Analysis Date = 11/10/11 Pct Recovery = 53% Analysis Date = 11/10/11 Pct Recovery = 53% Analysis Date = 10/30/11 Pct Recovery = 53% Analysis Date = 10/30/11 Pct Recovery = 53% Analysis Date = 10/20/11 Pct Recovery = 54% Analysis Date = 10/20/11 Pct Recovery = 54% Analysis Date = 10/09/11 Pct Recovery = 54% Analysis Date = 10/09/11 Pct Recovery = 54% Analysis Date = 09/28/11 Pct Recovery = 54% Analysis Date = 09/28/11 Pct Recovery = 54% Analysis Date = 09/18/11 Pct Recovery = 54% Analysis Date = 09/18/11 Pct Recovery = 54% Analysis Date = 09/07/11 Pct Recovery = 54% Analysis Date = 09/07/11 Pct Recovery = 54% Analysis Date = 08/27/11 Pct Recovery = 54% Analysis Date = 08/27/11 Pct Recovery = 54% Analysis Date = 08/17/11 Pct Recovery = 54% Analysis Date = 08/17/11 Pct Recovery = 54% Analysis Date = 08/06/11 Pct Recovery = 54% Analysis Date = 08/06/11 Pct Recovery = 54% Analysis Date = 07/26/11 Pct Recovery = 54% Analysis Date = 07/26/11 Pct Recovery = 54% Analysis Date = 07/16/11 Pct Recovery = 54% Analysis Date = 07/16/11 Pct Recovery = 54% Analysis Date = 07/05/11 Pct Recovery = 54% Analysis Date = 07/05/11 Pct Recovery = 54% Analysis Date = 06/24/11 Pct Recovery = 54% Analysis Date = 06/24/11 Pct Recovery = 54% Analysis Date = 06/14/11 Pct Recovery = 54% Analysis Date = 06/14/11 Pct Recovery = 54% Analysis Date = 06/03/11 Pct Recovery = 54% Analysis Date = 06/03/11 Pct Recovery = 54% Analysis Date = 05/23/11 Pct Recovery = 54% Analysis Date = 05/23/11 Pct Recovery = 54% Analysis Date = 05/13/11 Pct Recovery = 54% Analysis Date = 05/13/11 Pct Recovery = 54% Analysis Date = 05/02/11 Pct Recovery = 55% Analysis Date = 05/02/11 Pct Recovery = 55% Analysis Date = 04/21/11 Pct Recovery = 55% Analysis Date = 04/21/11 Pct Recovery = 55% Analysis Date = 04/11/11 Pct Recovery = 55% Analysis Date = 04/11/11 Pct Recovery = 55% Analysis Date = 03/31/11 Pct Recovery = 55% Analysis Date = 03/31/11 Pct Recovery = 55% Analysis Date = 03/20/11 Pct Recovery = 55% Analysis Date = 03/20/11 Pct Recovery = 55% Analysis Date = 03/10/11 Pct Recovery = 55% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
PROGESTERONE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 69 45% 15% 42% 12%
Total 69 45% 15% 42% 12%

Sample Statistics
PROGESTERONE

Characteristic N % % Basis
Plotted 69 87% Spiked
Estimated Values 69 87% Spiked
Deleted Values 2 2% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 81 .  
False Negatives 10 13% 10 out of 79
Not Spiked 50 .  
False Positives 0 0% 0 out of 50

BQS OBSP Determination:
TESTOSTERONE
METHOD: 4434 , TESTIDCODE: 64545GM005
Open Data Set

Analysis Date = 04/22/13 SpikeMix = ERA 0507-12-04.1: 50 µl & Restek A089631: 50 µl Pct Recovery = 77% Analysis Date = 04/03/13 SpikeMix = Spex Organics T1120525010: 50 µl & Restek A089631: 50 µl Pct Recovery = 76% Analysis Date = 02/22/13 SpikeMix = Restek A089631: 50 µl & Supelco LB92781: 50 µl Pct Recovery = 69% Analysis Date = 12/18/12 SpikeMix = ERA 0507-12-04.1: 50 µl & Restek A089631: 50 µl Pct Recovery = 81% Analysis Date = 12/03/12 SpikeMix = ERA 0511-12-02: 50 µl & Abs 051512: 50 µl Pct Recovery = 81% Analysis Date = 11/07/12 SpikeMix = ERA 0507-12-04.1: 50 µl & ERA 0511-12-02: 50 µl Pct Recovery = 86% Analysis Date = 03/27/12 SpikeMix = Crescent 162776: 100 µl Pct Recovery = 122% Analysis Date = 03/10/11 SpikeMix = Crescent 162776: 100 µl Pct Recovery = 79% Analysis Date = 06/23/11 SpikeMix = Crescent 162776: 100 µl Pct Recovery = 83% Analysis Date = 12/18/12 SpikeMix = Restek A089631: 25 µl & Supelco LB92781: 25 µl Pct Recovery = 82% Analysis Date = 04/10/13 SpikeMix = ERA 0511-12-02: 25 µl & Supelco LB92781: 25 µl Pct Recovery = 92% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120525010: 25 µl & ERA 0511-12-02: 25 µl Pct Recovery = 83% Analysis Date = 08/31/12 SpikeMix = ERA 0511-12-02: 25 µl & Abs 051512: 25 µl Pct Recovery = 86% Analysis Date = 03/14/14 SpikeMix = Supelco LB99393: 50 µl & Abs 050813: 50 µl Pct Recovery = 83% Analysis Date = 03/14/14 SpikeMix = Supelco LB99393: 50 µl & Abs 060413: 50 µl & Abs 071513: 50 µl Pct Recovery = 69% Analysis Date = 03/05/14 SpikeMix = ERA 0415-13-01.1A: 50 µl & Abs 060413: 50 µl & Abs 071513: 50 µl Pct Recovery = 74% Analysis Date = 02/25/14 SpikeMix = ERA 0415-13-01.1A: 50 µl & Abs 050813: 50 µl Pct Recovery = 70% Analysis Date = 12/15/16 SpikeMix = Abs 061416H: 50 µl & ChemService 5016100: 50 µl Pct Recovery = 83% Analysis Date = 04/13/15 SpikeMix = Abs 042114: 60 µl & Spex Organics E1140505004: 60 µl Pct Recovery = 60% Analysis Date = 04/01/15 SpikeMix = Spex Organics E1140505004: 60 µl & Supelco LC06946: 60 µl Pct Recovery = 56% Analysis Date = 01/21/15 SpikeMix = ChemService 2561700: 60 µl & Spex Organics E1140505004: 60 µl Pct Recovery = 54% Analysis Date = 12/09/14 SpikeMix = Abs 031014: 60 µl & Supelco LC06946: 60 µl Pct Recovery = 65% Analysis Date = 08/26/14 SpikeMix = Abs 031014: 60 µl & Abs 042114: 60 µl Pct Recovery = 81% Analysis Date = 08/11/14 SpikeMix = Abs 031014: 60 µl & ERA 0227-14-07.2: 60 µl Pct Recovery = 77% Analysis Date = 05/06/14 SpikeMix = Abs 031014: 60 µl & ChemService 2561700: 60 µl Pct Recovery = 73% Analysis Date = 01/08/16 SpikeMix = Spex Organics EN150501025: 60 µl & ERA 0601-15-04: 60 µl Pct Recovery = 72% Analysis Date = 01/05/16 SpikeMix = Supelco LC13547: 60 µl & ChemService 4073900: 60 µl Pct Recovery = 79% Analysis Date = 07/12/16 SpikeMix = Spex Organics EN150501025: 50 µl & ERA 0601-15-04: 50 µl Pct Recovery = 81% Analysis Date = 06/24/16 SpikeMix = ERA 0601-15-04: 50 µl & ChemService 4073900: 50 µl Pct Recovery = 74% Analysis Date = 12/10/15 SpikeMix = Abs 041515: 50 µl & ERA 0601-15-04: 50 µl Pct Recovery = 64% Analysis Date = 09/14/15 SpikeMix = ERA 0601-15-04: 50 µl & ChemService 4073900: 50 µl Pct Recovery = 72% Analysis Date = 08/10/15 SpikeMix = ERA 0601-15-04: 50 µl & Crescent 04EE007: 50 µl Pct Recovery = 86% Analysis Date = 07/21/15 SpikeMix = Supelco LC13547: 50 µl & Spex Organics EN150501025: 50 µl Pct Recovery = 76% Analysis Date = 12/05/16 SpikeMix = Abs 052616: 30 µl & Abs 061416H: 30 µl Pct Recovery = 100% Analysis Date = 04/01/15 SpikeMix = ChemService 2561700: 30 µl & Spex Organics E1140505004: 30 µl Pct Recovery = 68% Analysis Date = 01/29/15 SpikeMix = Abs 031014: 30 µl & Supelco LC06946: 30 µl Pct Recovery = 56% Analysis Date = 12/23/14 SpikeMix = Spex Organics E1140505004: 30 µl & Supelco LC06946: 30 µl Pct Recovery = 55% Analysis Date = 12/22/14 SpikeMix = Abs 042114: 30 µl & Abs 031014: 30 µl Pct Recovery = 78% Analysis Date = 09/04/14 SpikeMix = ERA 0227-14-07.2: 30 µl & Spex Organics E1140505004: 30 µl Pct Recovery = 61% Analysis Date = 07/14/14 SpikeMix = ERA 0227-14-07.2: 30 µl & Abs 031014: 30 µl Pct Recovery = 71% Analysis Date = 05/14/14 SpikeMix = Abs 031014: 30 µl & ChemService 2561700: 30 µl Pct Recovery = 80% Analysis Date = 03/03/14 SpikeMix = Abs 050813: 20 µl & Abs 071513: 20 µl Pct Recovery = 60% Analysis Date = 02/19/14 SpikeMix = Abs 050813: 20 µl & Abs 071513: 20 µl Pct Recovery = 68% Analysis Date = 01/23/14 SpikeMix = Supelco LB99393: 20 µl & ERA 0415-13-01.2A: 20 µl & Abs 060413: 20 µl Pct Recovery = 90% Analysis Date = 11/18/13 SpikeMix = ERA 0415-13-01.2A: 20 µl & Abs 050813: 20 µl Pct Recovery = 82% Analysis Date = 09/16/13 SpikeMix = ERA 0415-13-01.1A: 20 µl & ERA 0415-13-01.2A: 20 µl & Abs 060413: 20 µl Pct Recovery = 85% Analysis Date = 04/06/12 SpikeMix = Crescent 162776: 25 µl Pct Recovery = 91% Analysis Date = 11/17/11 SpikeMix = Crescent 162776: 25 µl Pct Recovery = 103% Analysis Date = 10/12/11 SpikeMix = Crescent 162776: 25 µl Pct Recovery = 92% Analysis Date = 07/25/11 SpikeMix = Crescent 162776: 25 µl Pct Recovery = 75% Analysis Date = 05/09/11 SpikeMix = Crescent 162776: 25 µl Pct Recovery = 76% Analysis Date = 01/08/16 SpikeMix = ERA 0601-15-04: 30 µl & ChemService 4073900: 30 µl Pct Recovery = 69% Analysis Date = 01/08/16 SpikeMix = ERA 0601-15-04: 30 µl & Crescent 04EE007: 30 µl Pct Recovery = 67% Analysis Date = 03/18/16 SpikeMix = Supelco LC13547: 30 µl & ChemService 4073900: 30 µl Pct Recovery = 85% Analysis Date = 03/18/16 SpikeMix = Spex Organics EN150501025: 30 µl & Supelco LC13547: 30 µl Pct Recovery = 98% Analysis Date = 12/14/16 Pct Recovery = 89% Analysis Date = 12/04/16 Pct Recovery = 89% Analysis Date = 12/04/16 Pct Recovery = 89% Analysis Date = 11/23/16 Pct Recovery = 88% Analysis Date = 11/23/16 Pct Recovery = 88% Analysis Date = 11/13/16 Pct Recovery = 88% Analysis Date = 11/13/16 Pct Recovery = 88% Analysis Date = 11/02/16 Pct Recovery = 87% Analysis Date = 11/02/16 Pct Recovery = 87% Analysis Date = 10/23/16 Pct Recovery = 87% Analysis Date = 10/23/16 Pct Recovery = 87% Analysis Date = 10/12/16 Pct Recovery = 87% Analysis Date = 10/12/16 Pct Recovery = 87% Analysis Date = 10/02/16 Pct Recovery = 86% Analysis Date = 10/02/16 Pct Recovery = 86% Analysis Date = 09/21/16 Pct Recovery = 86% Analysis Date = 09/21/16 Pct Recovery = 86% Analysis Date = 09/11/16 Pct Recovery = 85% Analysis Date = 09/11/16 Pct Recovery = 85% Analysis Date = 08/31/16 Pct Recovery = 85% Analysis Date = 08/31/16 Pct Recovery = 85% Analysis Date = 08/21/16 Pct Recovery = 85% Analysis Date = 08/21/16 Pct Recovery = 85% Analysis Date = 08/10/16 Pct Recovery = 84% Analysis Date = 08/10/16 Pct Recovery = 84% Analysis Date = 07/31/16 Pct Recovery = 84% Analysis Date = 07/31/16 Pct Recovery = 84% Analysis Date = 07/20/16 Pct Recovery = 84% Analysis Date = 07/20/16 Pct Recovery = 84% Analysis Date = 07/09/16 Pct Recovery = 83% Analysis Date = 07/09/16 Pct Recovery = 83% Analysis Date = 06/29/16 Pct Recovery = 83% Analysis Date = 06/29/16 Pct Recovery = 83% Analysis Date = 06/18/16 Pct Recovery = 82% Analysis Date = 06/18/16 Pct Recovery = 82% Analysis Date = 06/08/16 Pct Recovery = 82% Analysis Date = 06/08/16 Pct Recovery = 82% Analysis Date = 05/28/16 Pct Recovery = 82% Analysis Date = 05/28/16 Pct Recovery = 82% Analysis Date = 05/18/16 Pct Recovery = 81% Analysis Date = 05/18/16 Pct Recovery = 81% Analysis Date = 05/07/16 Pct Recovery = 81% Analysis Date = 05/07/16 Pct Recovery = 81% Analysis Date = 04/27/16 Pct Recovery = 80% Analysis Date = 04/27/16 Pct Recovery = 80% Analysis Date = 04/16/16 Pct Recovery = 80% Analysis Date = 04/16/16 Pct Recovery = 80% Analysis Date = 04/06/16 Pct Recovery = 80% Analysis Date = 04/06/16 Pct Recovery = 80% Analysis Date = 03/26/16 Pct Recovery = 79% Analysis Date = 03/26/16 Pct Recovery = 79% Analysis Date = 03/16/16 Pct Recovery = 79% Analysis Date = 03/16/16 Pct Recovery = 79% Analysis Date = 03/05/16 Pct Recovery = 78% Analysis Date = 03/05/16 Pct Recovery = 78% Analysis Date = 02/24/16 Pct Recovery = 78% Analysis Date = 02/24/16 Pct Recovery = 78% Analysis Date = 02/13/16 Pct Recovery = 78% Analysis Date = 02/13/16 Pct Recovery = 78% Analysis Date = 02/02/16 Pct Recovery = 77% Analysis Date = 02/02/16 Pct Recovery = 77% Analysis Date = 01/23/16 Pct Recovery = 77% Analysis Date = 01/23/16 Pct Recovery = 77% Analysis Date = 01/12/16 Pct Recovery = 77% Analysis Date = 01/12/16 Pct Recovery = 77% Analysis Date = 01/02/16 Pct Recovery = 76% Analysis Date = 01/02/16 Pct Recovery = 76% Analysis Date = 12/22/15 Pct Recovery = 76% Analysis Date = 12/22/15 Pct Recovery = 76% Analysis Date = 12/12/15 Pct Recovery = 75% Analysis Date = 12/12/15 Pct Recovery = 75% Analysis Date = 12/01/15 Pct Recovery = 75% Analysis Date = 12/01/15 Pct Recovery = 75% Analysis Date = 11/21/15 Pct Recovery = 75% Analysis Date = 11/21/15 Pct Recovery = 75% Analysis Date = 11/10/15 Pct Recovery = 74% Analysis Date = 11/10/15 Pct Recovery = 74% Analysis Date = 10/31/15 Pct Recovery = 74% Analysis Date = 10/31/15 Pct Recovery = 74% Analysis Date = 10/20/15 Pct Recovery = 74% Analysis Date = 10/20/15 Pct Recovery = 74% Analysis Date = 10/10/15 Pct Recovery = 73% Analysis Date = 10/10/15 Pct Recovery = 73% Analysis Date = 09/29/15 Pct Recovery = 73% Analysis Date = 09/29/15 Pct Recovery = 73% Analysis Date = 09/18/15 Pct Recovery = 73% Analysis Date = 09/18/15 Pct Recovery = 73% Analysis Date = 09/08/15 Pct Recovery = 72% Analysis Date = 09/08/15 Pct Recovery = 72% Analysis Date = 08/28/15 Pct Recovery = 72% Analysis Date = 08/28/15 Pct Recovery = 72% Analysis Date = 08/18/15 Pct Recovery = 71% Analysis Date = 08/18/15 Pct Recovery = 71% Analysis Date = 08/07/15 Pct Recovery = 71% Analysis Date = 08/07/15 Pct Recovery = 71% Analysis Date = 07/28/15 Pct Recovery = 71% Analysis Date = 07/28/15 Pct Recovery = 71% Analysis Date = 07/17/15 Pct Recovery = 70% Analysis Date = 07/17/15 Pct Recovery = 70% Analysis Date = 07/07/15 Pct Recovery = 70% Analysis Date = 07/07/15 Pct Recovery = 70% Analysis Date = 06/26/15 Pct Recovery = 70% Analysis Date = 06/26/15 Pct Recovery = 70% Analysis Date = 06/16/15 Pct Recovery = 70% Analysis Date = 06/16/15 Pct Recovery = 70% Analysis Date = 06/05/15 Pct Recovery = 70% Analysis Date = 06/05/15 Pct Recovery = 70% Analysis Date = 05/26/15 Pct Recovery = 70% Analysis Date = 05/26/15 Pct Recovery = 70% Analysis Date = 05/15/15 Pct Recovery = 69% Analysis Date = 05/15/15 Pct Recovery = 69% Analysis Date = 05/05/15 Pct Recovery = 69% Analysis Date = 05/05/15 Pct Recovery = 69% Analysis Date = 04/24/15 Pct Recovery = 69% Analysis Date = 04/24/15 Pct Recovery = 69% Analysis Date = 04/13/15 Pct Recovery = 69% Analysis Date = 04/13/15 Pct Recovery = 69% Analysis Date = 04/03/15 Pct Recovery = 69% Analysis Date = 04/03/15 Pct Recovery = 69% Analysis Date = 03/23/15 Pct Recovery = 69% Analysis Date = 03/23/15 Pct Recovery = 69% Analysis Date = 03/13/15 Pct Recovery = 69% Analysis Date = 03/13/15 Pct Recovery = 69% Analysis Date = 03/02/15 Pct Recovery = 68% Analysis Date = 03/02/15 Pct Recovery = 68% Analysis Date = 02/20/15 Pct Recovery = 68% Analysis Date = 02/20/15 Pct Recovery = 68% Analysis Date = 02/09/15 Pct Recovery = 68% Analysis Date = 02/09/15 Pct Recovery = 68% Analysis Date = 01/30/15 Pct Recovery = 68% Analysis Date = 01/30/15 Pct Recovery = 68% Analysis Date = 01/19/15 Pct Recovery = 68% Analysis Date = 01/19/15 Pct Recovery = 68% Analysis Date = 01/09/15 Pct Recovery = 68% Analysis Date = 01/09/15 Pct Recovery = 68% Analysis Date = 12/29/14 Pct Recovery = 68% Analysis Date = 12/29/14 Pct Recovery = 68% Analysis Date = 12/19/14 Pct Recovery = 68% Analysis Date = 12/19/14 Pct Recovery = 68% Analysis Date = 12/08/14 Pct Recovery = 68% Analysis Date = 12/08/14 Pct Recovery = 68% Analysis Date = 11/28/14 Pct Recovery = 69% Analysis Date = 11/28/14 Pct Recovery = 69% Analysis Date = 11/17/14 Pct Recovery = 69% Analysis Date = 11/17/14 Pct Recovery = 69% Analysis Date = 11/06/14 Pct Recovery = 69% Analysis Date = 11/06/14 Pct Recovery = 69% Analysis Date = 10/27/14 Pct Recovery = 69% Analysis Date = 10/27/14 Pct Recovery = 69% Analysis Date = 10/16/14 Pct Recovery = 69% Analysis Date = 10/16/14 Pct Recovery = 69% Analysis Date = 10/06/14 Pct Recovery = 69% Analysis Date = 10/06/14 Pct Recovery = 69% Analysis Date = 09/25/14 Pct Recovery = 69% Analysis Date = 09/25/14 Pct Recovery = 69% Analysis Date = 09/15/14 Pct Recovery = 70% Analysis Date = 09/15/14 Pct Recovery = 70% Analysis Date = 09/04/14 Pct Recovery = 70% Analysis Date = 09/04/14 Pct Recovery = 70% Analysis Date = 08/25/14 Pct Recovery = 70% Analysis Date = 08/25/14 Pct Recovery = 70% Analysis Date = 08/14/14 Pct Recovery = 70% Analysis Date = 08/14/14 Pct Recovery = 70% Analysis Date = 08/04/14 Pct Recovery = 70% Analysis Date = 08/04/14 Pct Recovery = 70% Analysis Date = 07/24/14 Pct Recovery = 71% Analysis Date = 07/24/14 Pct Recovery = 71% Analysis Date = 07/14/14 Pct Recovery = 71% Analysis Date = 07/14/14 Pct Recovery = 71% Analysis Date = 07/03/14 Pct Recovery = 71% Analysis Date = 07/03/14 Pct Recovery = 71% Analysis Date = 06/22/14 Pct Recovery = 72% Analysis Date = 06/22/14 Pct Recovery = 72% Analysis Date = 06/12/14 Pct Recovery = 72% Analysis Date = 06/12/14 Pct Recovery = 72% Analysis Date = 06/01/14 Pct Recovery = 72% Analysis Date = 06/01/14 Pct Recovery = 72% Analysis Date = 05/22/14 Pct Recovery = 73% Analysis Date = 05/22/14 Pct Recovery = 73% Analysis Date = 05/11/14 Pct Recovery = 73% Analysis Date = 05/11/14 Pct Recovery = 73% Analysis Date = 05/01/14 Pct Recovery = 73% Analysis Date = 05/01/14 Pct Recovery = 73% Analysis Date = 04/20/14 Pct Recovery = 73% Analysis Date = 04/20/14 Pct Recovery = 73% Analysis Date = 04/10/14 Pct Recovery = 74% Analysis Date = 04/10/14 Pct Recovery = 74% Analysis Date = 03/30/14 Pct Recovery = 74% Analysis Date = 03/30/14 Pct Recovery = 74% Analysis Date = 03/20/14 Pct Recovery = 74% Analysis Date = 03/20/14 Pct Recovery = 74% Analysis Date = 03/09/14 Pct Recovery = 75% Analysis Date = 03/09/14 Pct Recovery = 75% Analysis Date = 02/27/14 Pct Recovery = 75% Analysis Date = 02/27/14 Pct Recovery = 75% Analysis Date = 02/16/14 Pct Recovery = 75% Analysis Date = 02/16/14 Pct Recovery = 75% Analysis Date = 02/06/14 Pct Recovery = 75% Analysis Date = 02/06/14 Pct Recovery = 75% Analysis Date = 01/26/14 Pct Recovery = 75% Analysis Date = 01/26/14 Pct Recovery = 75% Analysis Date = 01/15/14 Pct Recovery = 76% Analysis Date = 01/15/14 Pct Recovery = 76% Analysis Date = 01/05/14 Pct Recovery = 76% Analysis Date = 01/05/14 Pct Recovery = 76% Analysis Date = 12/25/13 Pct Recovery = 76% Analysis Date = 12/25/13 Pct Recovery = 76% Analysis Date = 12/15/13 Pct Recovery = 76% Analysis Date = 12/15/13 Pct Recovery = 76% Analysis Date = 12/04/13 Pct Recovery = 77% Analysis Date = 12/04/13 Pct Recovery = 77% Analysis Date = 11/24/13 Pct Recovery = 77% Analysis Date = 11/24/13 Pct Recovery = 77% Analysis Date = 11/13/13 Pct Recovery = 77% Analysis Date = 11/13/13 Pct Recovery = 77% Analysis Date = 11/03/13 Pct Recovery = 77% Analysis Date = 11/03/13 Pct Recovery = 77% Analysis Date = 10/23/13 Pct Recovery = 78% Analysis Date = 10/23/13 Pct Recovery = 78% Analysis Date = 10/13/13 Pct Recovery = 78% Analysis Date = 10/13/13 Pct Recovery = 78% Analysis Date = 10/02/13 Pct Recovery = 78% Analysis Date = 10/02/13 Pct Recovery = 78% Analysis Date = 09/22/13 Pct Recovery = 78% Analysis Date = 09/22/13 Pct Recovery = 78% Analysis Date = 09/11/13 Pct Recovery = 79% Analysis Date = 09/11/13 Pct Recovery = 79% Analysis Date = 09/01/13 Pct Recovery = 79% Analysis Date = 09/01/13 Pct Recovery = 79% Analysis Date = 08/21/13 Pct Recovery = 79% Analysis Date = 08/21/13 Pct Recovery = 79% Analysis Date = 08/10/13 Pct Recovery = 79% Analysis Date = 08/10/13 Pct Recovery = 79% Analysis Date = 07/31/13 Pct Recovery = 80% Analysis Date = 07/31/13 Pct Recovery = 80% Analysis Date = 07/20/13 Pct Recovery = 80% Analysis Date = 07/20/13 Pct Recovery = 80% Analysis Date = 07/10/13 Pct Recovery = 80% Analysis Date = 07/10/13 Pct Recovery = 80% Analysis Date = 06/29/13 Pct Recovery = 80% Analysis Date = 06/29/13 Pct Recovery = 80% Analysis Date = 06/19/13 Pct Recovery = 81% Analysis Date = 06/19/13 Pct Recovery = 81% Analysis Date = 06/08/13 Pct Recovery = 81% Analysis Date = 06/08/13 Pct Recovery = 81% Analysis Date = 05/29/13 Pct Recovery = 81% Analysis Date = 05/29/13 Pct Recovery = 81% Analysis Date = 05/18/13 Pct Recovery = 81% Analysis Date = 05/18/13 Pct Recovery = 81% Analysis Date = 05/08/13 Pct Recovery = 82% Analysis Date = 05/08/13 Pct Recovery = 82% Analysis Date = 04/27/13 Pct Recovery = 82% Analysis Date = 04/27/13 Pct Recovery = 82% Analysis Date = 04/17/13 Pct Recovery = 82% Analysis Date = 04/17/13 Pct Recovery = 82% Analysis Date = 04/06/13 Pct Recovery = 82% Analysis Date = 04/06/13 Pct Recovery = 82% Analysis Date = 03/26/13 Pct Recovery = 83% Analysis Date = 03/26/13 Pct Recovery = 83% Analysis Date = 03/16/13 Pct Recovery = 83% Analysis Date = 03/16/13 Pct Recovery = 83% Analysis Date = 03/05/13 Pct Recovery = 83% Analysis Date = 03/05/13 Pct Recovery = 83% Analysis Date = 02/23/13 Pct Recovery = 84% Analysis Date = 02/23/13 Pct Recovery = 84% Analysis Date = 02/12/13 Pct Recovery = 84% Analysis Date = 02/12/13 Pct Recovery = 84% Analysis Date = 02/02/13 Pct Recovery = 84% Analysis Date = 02/02/13 Pct Recovery = 84% Analysis Date = 01/22/13 Pct Recovery = 85% Analysis Date = 01/22/13 Pct Recovery = 85% Analysis Date = 01/12/13 Pct Recovery = 85% Analysis Date = 01/12/13 Pct Recovery = 85% Analysis Date = 01/01/13 Pct Recovery = 85% Analysis Date = 01/01/13 Pct Recovery = 85% Analysis Date = 12/22/12 Pct Recovery = 85% Analysis Date = 12/22/12 Pct Recovery = 85% Analysis Date = 12/11/12 Pct Recovery = 86% Analysis Date = 12/11/12 Pct Recovery = 86% Analysis Date = 12/01/12 Pct Recovery = 86% Analysis Date = 12/01/12 Pct Recovery = 86% Analysis Date = 11/20/12 Pct Recovery = 86% Analysis Date = 11/20/12 Pct Recovery = 86% Analysis Date = 11/10/12 Pct Recovery = 86% Analysis Date = 11/10/12 Pct Recovery = 86% Analysis Date = 10/30/12 Pct Recovery = 86% Analysis Date = 10/30/12 Pct Recovery = 86% Analysis Date = 10/19/12 Pct Recovery = 86% Analysis Date = 10/19/12 Pct Recovery = 86% Analysis Date = 10/09/12 Pct Recovery = 86% Analysis Date = 10/09/12 Pct Recovery = 86% Analysis Date = 09/28/12 Pct Recovery = 86% Analysis Date = 09/28/12 Pct Recovery = 86% Analysis Date = 09/18/12 Pct Recovery = 86% Analysis Date = 09/18/12 Pct Recovery = 86% Analysis Date = 09/07/12 Pct Recovery = 86% Analysis Date = 09/07/12 Pct Recovery = 86% Analysis Date = 08/28/12 Pct Recovery = 86% Analysis Date = 08/28/12 Pct Recovery = 86% Analysis Date = 08/17/12 Pct Recovery = 86% Analysis Date = 08/17/12 Pct Recovery = 86% Analysis Date = 08/07/12 Pct Recovery = 86% Analysis Date = 08/07/12 Pct Recovery = 86% Analysis Date = 07/27/12 Pct Recovery = 86% Analysis Date = 07/27/12 Pct Recovery = 86% Analysis Date = 07/17/12 Pct Recovery = 86% Analysis Date = 07/17/12 Pct Recovery = 86% Analysis Date = 07/06/12 Pct Recovery = 86% Analysis Date = 07/06/12 Pct Recovery = 86% Analysis Date = 06/26/12 Pct Recovery = 86% Analysis Date = 06/26/12 Pct Recovery = 86% Analysis Date = 06/15/12 Pct Recovery = 86% Analysis Date = 06/15/12 Pct Recovery = 86% Analysis Date = 06/05/12 Pct Recovery = 86% Analysis Date = 06/05/12 Pct Recovery = 86% Analysis Date = 05/25/12 Pct Recovery = 86% Analysis Date = 05/25/12 Pct Recovery = 86% Analysis Date = 05/14/12 Pct Recovery = 86% Analysis Date = 05/14/12 Pct Recovery = 86% Analysis Date = 05/04/12 Pct Recovery = 86% Analysis Date = 05/04/12 Pct Recovery = 86% Analysis Date = 04/23/12 Pct Recovery = 86% Analysis Date = 04/23/12 Pct Recovery = 86% Analysis Date = 04/13/12 Pct Recovery = 86% Analysis Date = 04/13/12 Pct Recovery = 86% Analysis Date = 04/02/12 Pct Recovery = 86% Analysis Date = 04/02/12 Pct Recovery = 86% Analysis Date = 03/23/12 Pct Recovery = 86% Analysis Date = 03/23/12 Pct Recovery = 86% Analysis Date = 03/12/12 Pct Recovery = 86% Analysis Date = 03/12/12 Pct Recovery = 86% Analysis Date = 03/02/12 Pct Recovery = 86% Analysis Date = 03/02/12 Pct Recovery = 86% Analysis Date = 02/20/12 Pct Recovery = 86% Analysis Date = 02/20/12 Pct Recovery = 86% Analysis Date = 02/10/12 Pct Recovery = 86% Analysis Date = 02/10/12 Pct Recovery = 86% Analysis Date = 01/30/12 Pct Recovery = 87% Analysis Date = 01/30/12 Pct Recovery = 87% Analysis Date = 01/20/12 Pct Recovery = 87% Analysis Date = 01/20/12 Pct Recovery = 87% Analysis Date = 01/09/12 Pct Recovery = 87% Analysis Date = 01/09/12 Pct Recovery = 87% Analysis Date = 12/29/11 Pct Recovery = 87% Analysis Date = 12/29/11 Pct Recovery = 87% Analysis Date = 12/19/11 Pct Recovery = 87% Analysis Date = 12/19/11 Pct Recovery = 87% Analysis Date = 12/08/11 Pct Recovery = 87% Analysis Date = 12/08/11 Pct Recovery = 87% Analysis Date = 11/28/11 Pct Recovery = 87% Analysis Date = 11/28/11 Pct Recovery = 87% Analysis Date = 11/17/11 Pct Recovery = 87% Analysis Date = 11/17/11 Pct Recovery = 87% Analysis Date = 11/07/11 Pct Recovery = 87% Analysis Date = 11/07/11 Pct Recovery = 87% Analysis Date = 10/27/11 Pct Recovery = 87% Analysis Date = 10/27/11 Pct Recovery = 87% Analysis Date = 10/17/11 Pct Recovery = 87% Analysis Date = 10/17/11 Pct Recovery = 87% Analysis Date = 10/06/11 Pct Recovery = 87% Analysis Date = 10/06/11 Pct Recovery = 87% Analysis Date = 09/26/11 Pct Recovery = 87% Analysis Date = 09/26/11 Pct Recovery = 87% Analysis Date = 09/15/11 Pct Recovery = 87% Analysis Date = 09/15/11 Pct Recovery = 87% Analysis Date = 09/05/11 Pct Recovery = 87% Analysis Date = 09/05/11 Pct Recovery = 87% Analysis Date = 08/25/11 Pct Recovery = 87% Analysis Date = 08/25/11 Pct Recovery = 87% Analysis Date = 08/15/11 Pct Recovery = 87% Analysis Date = 08/15/11 Pct Recovery = 87% Analysis Date = 08/04/11 Pct Recovery = 87% Analysis Date = 08/04/11 Pct Recovery = 87% Analysis Date = 07/24/11 Pct Recovery = 87% Analysis Date = 07/24/11 Pct Recovery = 87% Analysis Date = 07/14/11 Pct Recovery = 87% Analysis Date = 07/14/11 Pct Recovery = 87% Analysis Date = 07/03/11 Pct Recovery = 87% Analysis Date = 07/03/11 Pct Recovery = 87% Analysis Date = 06/23/11 Pct Recovery = 87% Analysis Date = 06/23/11 Pct Recovery = 87% Analysis Date = 06/12/11 Pct Recovery = 88% Analysis Date = 06/12/11 Pct Recovery = 88% Analysis Date = 06/02/11 Pct Recovery = 88% Analysis Date = 06/02/11 Pct Recovery = 88% Analysis Date = 05/22/11 Pct Recovery = 88% Analysis Date = 05/22/11 Pct Recovery = 88% Analysis Date = 05/12/11 Pct Recovery = 88% Analysis Date = 05/12/11 Pct Recovery = 88% Analysis Date = 05/01/11 Pct Recovery = 88% Analysis Date = 05/01/11 Pct Recovery = 88% Analysis Date = 04/21/11 Pct Recovery = 88% Analysis Date = 04/21/11 Pct Recovery = 88% Analysis Date = 04/10/11 Pct Recovery = 88% Analysis Date = 04/10/11 Pct Recovery = 88% Analysis Date = 03/31/11 Pct Recovery = 88% Analysis Date = 03/31/11 Pct Recovery = 88% Analysis Date = 03/20/11 Pct Recovery = 88% Analysis Date = 03/20/11 Pct Recovery = 88% Analysis Date = 03/10/11 Pct Recovery = 88% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
TESTOSTERONE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 55 77% 13% 77% 10%
Total 55 77% 13% 77% 10%

Sample Statistics
TESTOSTERONE

Characteristic N % % Basis
Plotted 55 89% Spiked
Estimated Values 0 0% Spiked
Deleted Values 2 2% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 63 .  
False Negatives 7 11% 7 out of 62
Not Spiked 68 .  
False Positives 3 4% 3 out of 67

BQS OBSP Determination:
TRANS-DIETHYLSTILBESTROL
METHOD: 4434 , TESTIDCODE: 64536GM005
Open Data Set

Analysis Date = 08/31/16 SpikeMix = Spex Organics TS160420010: 50 µl & ChemService 5016200: 50 µl Pct Recovery = 57% Analysis Date = 08/19/16 SpikeMix = Supelco LC20140V: 50 µl & Spex Organics TS160420010: 50 µl Pct Recovery = 57% Analysis Date = 08/11/16 SpikeMix = ChemService 5016100: 50 µl & Spex Organics TS160420010: 50 µl Pct Recovery = 48% Analysis Date = 03/27/12 SpikeMix = Crescent 162776: 100 µl Pct Recovery = 59% Analysis Date = 12/03/12 SpikeMix = ERA 0511-12-02: 50 µl & Abs 051512: 50 µl Pct Recovery = 56% Analysis Date = 11/07/12 SpikeMix = ERA 0507-12-04.1: 50 µl & ERA 0511-12-02: 50 µl Pct Recovery = 51% Analysis Date = 04/22/13 SpikeMix = ERA 0507-12-04.1: 50 µl & Restek A089631: 50 µl Pct Recovery = 60% Analysis Date = 04/03/13 SpikeMix = Spex Organics T1120525010: 50 µl & Restek A089631: 50 µl Pct Recovery = 78% Analysis Date = 02/22/13 SpikeMix = Restek A089631: 50 µl & Supelco LB92781: 50 µl Pct Recovery = 73% Analysis Date = 12/18/12 SpikeMix = ERA 0507-12-04.1: 50 µl & Restek A089631: 50 µl Pct Recovery = 58% Analysis Date = 01/27/12 SpikeMix = Supelco LB77167: 100 µl Pct Recovery = 58% Analysis Date = 10/13/11 SpikeMix = Supelco LB77167: 100 µl Pct Recovery = 50% Analysis Date = 03/10/11 SpikeMix = Crescent 162776: 100 µl Pct Recovery = 67% Analysis Date = 06/07/11 SpikeMix = Supelco LB77167: 100 µl Pct Recovery = 58% Analysis Date = 06/23/11 SpikeMix = Crescent 162776: 100 µl Pct Recovery = 66% Analysis Date = 04/14/14 SpikeMix = ERA 0415-13-01.1A: 50 µl & Abs 071513: 50 µl Pct Recovery = 83% Analysis Date = 03/05/14 SpikeMix = ERA 0415-13-01.1A: 50 µl & Abs 060413: 50 µl & Abs 071513: 50 µl Pct Recovery = 76% Analysis Date = 03/05/14 SpikeMix = Spex Organics T1130423008: 50 µl & Abs 071513: 50 µl Pct Recovery = 73% Analysis Date = 08/09/13 SpikeMix = ERA 0415-13-01.2A: 50 µl & Spex Organics T1130423008: 50 µl Pct Recovery = 69% Analysis Date = 04/10/13 SpikeMix = ERA 0511-12-02: 25 µl & Supelco LB92781: 25 µl Pct Recovery = 69% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120525010: 25 µl & ERA 0511-12-02: 25 µl Pct Recovery = 74% Analysis Date = 08/31/12 SpikeMix = ERA 0511-12-02: 25 µl & Abs 051512: 25 µl Pct Recovery = 71% Analysis Date = 04/13/15 SpikeMix = Abs 042114: 60 µl & Spex Organics E1140505004: 60 µl Pct Recovery = 71% Analysis Date = 04/01/15 SpikeMix = Spex Organics E1140505004: 60 µl & Supelco LC06946: 60 µl Pct Recovery = 52% Analysis Date = 01/21/15 SpikeMix = ChemService 2561700: 60 µl & Spex Organics E1140505004: 60 µl Pct Recovery = 64% Analysis Date = 12/09/14 SpikeMix = Abs 031014: 60 µl & Supelco LC06946: 60 µl Pct Recovery = 57% Analysis Date = 08/26/14 SpikeMix = Abs 031014: 60 µl & Abs 042114: 60 µl Pct Recovery = 83% Analysis Date = 12/18/12 SpikeMix = Restek A089631: 25 µl & Supelco LB92781: 25 µl Pct Recovery = 54% Analysis Date = 01/07/16 SpikeMix = Crescent 04EE007: 60 µl & Abs 041515: 60 µl Pct Recovery = 51% Analysis Date = 01/05/16 SpikeMix = Supelco LC13547: 60 µl & ChemService 4073900: 60 µl Pct Recovery = 68% Analysis Date = 02/01/17 SpikeMix = Supelco LC20140V: 30 µl & Abs 052616: 30 µl Pct Recovery = 64% Analysis Date = 01/13/17 SpikeMix = Abs 052616: 30 µl & ChemService 5016200: 30 µl Pct Recovery = 74% Analysis Date = 12/29/16 SpikeMix = ChemService 5016100: 30 µl & Abs 052616: 30 µl Pct Recovery = 64% Analysis Date = 06/24/16 SpikeMix = ERA 0601-15-04: 50 µl & ChemService 4073900: 50 µl Pct Recovery = 70% Analysis Date = 01/08/16 SpikeMix = Crescent 04EE007: 50 µl & Spex Organics EN150501025: 50 µl Pct Recovery = 80% Analysis Date = 09/14/15 SpikeMix = ERA 0601-15-04: 50 µl & ChemService 4073900: 50 µl Pct Recovery = 81% Analysis Date = 08/17/15 SpikeMix = ChemService 4073900: 50 µl & Abs 041515: 50 µl Pct Recovery = 60% Analysis Date = 08/10/15 SpikeMix = ERA 0601-15-04: 50 µl & Crescent 04EE007: 50 µl Pct Recovery = 67% Analysis Date = 04/06/12 SpikeMix = Crescent 162776: 25 µl Pct Recovery = 80% Analysis Date = 11/17/11 SpikeMix = Crescent 162776: 25 µl Pct Recovery = 59% Analysis Date = 10/12/11 SpikeMix = Crescent 162776: 25 µl Pct Recovery = 55% Analysis Date = 07/25/11 SpikeMix = Crescent 162776: 25 µl Pct Recovery = 51% Analysis Date = 06/03/15 SpikeMix = Abs 031014: 30 µl & ERA 0227-14-07.2: 30 µl Pct Recovery = 68% Analysis Date = 04/01/15 SpikeMix = ChemService 2561700: 30 µl & Spex Organics E1140505004: 30 µl Pct Recovery = 69% Analysis Date = 01/29/15 SpikeMix = Abs 031014: 30 µl & Supelco LC06946: 30 µl Pct Recovery = 47% Analysis Date = 12/23/14 SpikeMix = Spex Organics E1140505004: 30 µl & Supelco LC06946: 30 µl Pct Recovery = 51% Analysis Date = 12/22/14 SpikeMix = Abs 042114: 30 µl & Abs 031014: 30 µl Pct Recovery = 83% Analysis Date = 09/04/14 SpikeMix = ERA 0227-14-07.2: 30 µl & Spex Organics E1140505004: 30 µl Pct Recovery = 56% Analysis Date = 07/14/14 SpikeMix = ERA 0227-14-07.2: 30 µl & Abs 031014: 30 µl Pct Recovery = 79% Analysis Date = 07/27/12 SpikeMix = Supelco LB77167: 25 µl Pct Recovery = 48% Analysis Date = 04/17/12 SpikeMix = Supelco LB77167: 25 µl Pct Recovery = 57% Analysis Date = 04/04/12 SpikeMix = Supelco LB77167: 25 µl Pct Recovery = 53% Analysis Date = 09/29/11 SpikeMix = Supelco LB77167: 25 µl Pct Recovery = 57% Analysis Date = 05/19/11 SpikeMix = Supelco LB77167: 25 µl Pct Recovery = 64% Analysis Date = 05/09/11 SpikeMix = Crescent 162776: 25 µl Pct Recovery = 59% Analysis Date = 03/31/11 SpikeMix = Supelco LB77167: 25 µl Pct Recovery = 65% Analysis Date = 03/03/14 SpikeMix = Abs 050813: 20 µl & Abs 071513: 20 µl Pct Recovery = 75% Analysis Date = 02/19/14 SpikeMix = Abs 050813: 20 µl & Abs 071513: 20 µl Pct Recovery = 62% Analysis Date = 01/23/14 SpikeMix = Supelco LB99393: 20 µl & ERA 0415-13-01.2A: 20 µl & Abs 060413: 20 µl Pct Recovery = 58% Analysis Date = 11/18/13 SpikeMix = ERA 0415-13-01.2A: 20 µl & Abs 050813: 20 µl Pct Recovery = 60% Analysis Date = 09/16/13 SpikeMix = ERA 0415-13-01.1A: 20 µl & ERA 0415-13-01.2A: 20 µl & Abs 060413: 20 µl Pct Recovery = 55% Analysis Date = 07/19/13 SpikeMix = Supelco LB99393: 20 µl & ERA 0415-13-01.2A: 20 µl Pct Recovery = 55% Analysis Date = 03/18/16 SpikeMix = Crescent 04EE007: 30 µl & Spex Organics EN150501025: 30 µl Pct Recovery = 86% Analysis Date = 03/07/16 SpikeMix = ChemService 4073900: 30 µl & Abs 041515: 30 µl Pct Recovery = 78% Analysis Date = 01/08/16 SpikeMix = ERA 0601-15-04: 30 µl & ChemService 4073900: 30 µl Pct Recovery = 80% Analysis Date = 01/08/16 SpikeMix = ERA 0601-15-04: 30 µl & Crescent 04EE007: 30 µl Pct Recovery = 105% Analysis Date = 12/11/15 SpikeMix = Crescent 04EE007: 30 µl & Spex Organics EN150501025: 30 µl Pct Recovery = 74% Analysis Date = 11/02/15 SpikeMix = Supelco LC13547: 30 µl & Crescent 04EE007: 30 µl Pct Recovery = 80% Analysis Date = 09/23/15 SpikeMix = ChemService 4073900: 30 µl & Spex Organics EN150501025: 30 µl Pct Recovery = 68% Analysis Date = 02/01/17 Pct Recovery = 68% Analysis Date = 01/21/17 Pct Recovery = 68% Analysis Date = 01/21/17 Pct Recovery = 68% Analysis Date = 01/10/17 Pct Recovery = 68% Analysis Date = 01/10/17 Pct Recovery = 68% Analysis Date = 12/30/16 Pct Recovery = 68% Analysis Date = 12/30/16 Pct Recovery = 68% Analysis Date = 12/19/16 Pct Recovery = 68% Analysis Date = 12/19/16 Pct Recovery = 68% Analysis Date = 12/09/16 Pct Recovery = 68% Analysis Date = 12/09/16 Pct Recovery = 68% Analysis Date = 11/28/16 Pct Recovery = 68% Analysis Date = 11/28/16 Pct Recovery = 68% Analysis Date = 11/17/16 Pct Recovery = 68% Analysis Date = 11/17/16 Pct Recovery = 68% Analysis Date = 11/06/16 Pct Recovery = 68% Analysis Date = 11/06/16 Pct Recovery = 68% Analysis Date = 10/27/16 Pct Recovery = 68% Analysis Date = 10/27/16 Pct Recovery = 68% Analysis Date = 10/16/16 Pct Recovery = 68% Analysis Date = 10/16/16 Pct Recovery = 68% Analysis Date = 10/05/16 Pct Recovery = 68% Analysis Date = 10/05/16 Pct Recovery = 68% Analysis Date = 09/24/16 Pct Recovery = 68% Analysis Date = 09/24/16 Pct Recovery = 68% Analysis Date = 09/13/16 Pct Recovery = 68% Analysis Date = 09/13/16 Pct Recovery = 68% Analysis Date = 09/03/16 Pct Recovery = 68% Analysis Date = 09/03/16 Pct Recovery = 68% Analysis Date = 08/23/16 Pct Recovery = 69% Analysis Date = 08/23/16 Pct Recovery = 69% Analysis Date = 08/12/16 Pct Recovery = 69% Analysis Date = 08/12/16 Pct Recovery = 69% Analysis Date = 08/01/16 Pct Recovery = 69% Analysis Date = 08/01/16 Pct Recovery = 69% Analysis Date = 07/22/16 Pct Recovery = 69% Analysis Date = 07/22/16 Pct Recovery = 69% Analysis Date = 07/11/16 Pct Recovery = 69% Analysis Date = 07/11/16 Pct Recovery = 69% Analysis Date = 06/30/16 Pct Recovery = 69% Analysis Date = 06/30/16 Pct Recovery = 69% Analysis Date = 06/19/16 Pct Recovery = 69% Analysis Date = 06/19/16 Pct Recovery = 69% Analysis Date = 06/08/16 Pct Recovery = 69% Analysis Date = 06/08/16 Pct Recovery = 69% Analysis Date = 05/29/16 Pct Recovery = 69% Analysis Date = 05/29/16 Pct Recovery = 69% Analysis Date = 05/18/16 Pct Recovery = 69% Analysis Date = 05/18/16 Pct Recovery = 69% Analysis Date = 05/07/16 Pct Recovery = 69% Analysis Date = 05/07/16 Pct Recovery = 69% Analysis Date = 04/26/16 Pct Recovery = 69% Analysis Date = 04/26/16 Pct Recovery = 69% Analysis Date = 04/16/16 Pct Recovery = 69% Analysis Date = 04/16/16 Pct Recovery = 69% Analysis Date = 04/05/16 Pct Recovery = 69% Analysis Date = 04/05/16 Pct Recovery = 69% Analysis Date = 03/25/16 Pct Recovery = 69% Analysis Date = 03/25/16 Pct Recovery = 69% Analysis Date = 03/14/16 Pct Recovery = 69% Analysis Date = 03/14/16 Pct Recovery = 69% Analysis Date = 03/03/16 Pct Recovery = 69% Analysis Date = 03/03/16 Pct Recovery = 69% Analysis Date = 02/22/16 Pct Recovery = 69% Analysis Date = 02/22/16 Pct Recovery = 69% Analysis Date = 02/11/16 Pct Recovery = 69% Analysis Date = 02/11/16 Pct Recovery = 69% Analysis Date = 01/31/16 Pct Recovery = 69% Analysis Date = 01/31/16 Pct Recovery = 69% Analysis Date = 01/20/16 Pct Recovery = 69% Analysis Date = 01/20/16 Pct Recovery = 69% Analysis Date = 01/10/16 Pct Recovery = 69% Analysis Date = 01/10/16 Pct Recovery = 69% Analysis Date = 12/30/15 Pct Recovery = 69% Analysis Date = 12/30/15 Pct Recovery = 69% Analysis Date = 12/19/15 Pct Recovery = 69% Analysis Date = 12/19/15 Pct Recovery = 69% Analysis Date = 12/08/15 Pct Recovery = 69% Analysis Date = 12/08/15 Pct Recovery = 69% Analysis Date = 11/28/15 Pct Recovery = 69% Analysis Date = 11/28/15 Pct Recovery = 69% Analysis Date = 11/17/15 Pct Recovery = 69% Analysis Date = 11/17/15 Pct Recovery = 69% Analysis Date = 11/06/15 Pct Recovery = 69% Analysis Date = 11/06/15 Pct Recovery = 69% Analysis Date = 10/26/15 Pct Recovery = 69% Analysis Date = 10/26/15 Pct Recovery = 69% Analysis Date = 10/15/15 Pct Recovery = 69% Analysis Date = 10/15/15 Pct Recovery = 69% Analysis Date = 10/05/15 Pct Recovery = 69% Analysis Date = 10/05/15 Pct Recovery = 69% Analysis Date = 09/24/15 Pct Recovery = 69% Analysis Date = 09/24/15 Pct Recovery = 69% Analysis Date = 09/13/15 Pct Recovery = 69% Analysis Date = 09/13/15 Pct Recovery = 69% Analysis Date = 09/02/15 Pct Recovery = 69% Analysis Date = 09/02/15 Pct Recovery = 69% Analysis Date = 08/23/15 Pct Recovery = 69% Analysis Date = 08/23/15 Pct Recovery = 69% Analysis Date = 08/12/15 Pct Recovery = 69% Analysis Date = 08/12/15 Pct Recovery = 69% Analysis Date = 08/01/15 Pct Recovery = 69% Analysis Date = 08/01/15 Pct Recovery = 69% Analysis Date = 07/21/15 Pct Recovery = 69% Analysis Date = 07/21/15 Pct Recovery = 69% Analysis Date = 07/10/15 Pct Recovery = 69% Analysis Date = 07/10/15 Pct Recovery = 69% Analysis Date = 06/30/15 Pct Recovery = 69% Analysis Date = 06/30/15 Pct Recovery = 69% Analysis Date = 06/19/15 Pct Recovery = 69% Analysis Date = 06/19/15 Pct Recovery = 69% Analysis Date = 06/08/15 Pct Recovery = 69% Analysis Date = 06/08/15 Pct Recovery = 69% Analysis Date = 05/28/15 Pct Recovery = 69% Analysis Date = 05/28/15 Pct Recovery = 69% Analysis Date = 05/18/15 Pct Recovery = 69% Analysis Date = 05/18/15 Pct Recovery = 69% Analysis Date = 05/07/15 Pct Recovery = 69% Analysis Date = 05/07/15 Pct Recovery = 69% Analysis Date = 04/26/15 Pct Recovery = 69% Analysis Date = 04/26/15 Pct Recovery = 69% Analysis Date = 04/15/15 Pct Recovery = 69% Analysis Date = 04/15/15 Pct Recovery = 69% Analysis Date = 04/04/15 Pct Recovery = 69% Analysis Date = 04/04/15 Pct Recovery = 69% Analysis Date = 03/25/15 Pct Recovery = 69% Analysis Date = 03/25/15 Pct Recovery = 69% Analysis Date = 03/14/15 Pct Recovery = 69% Analysis Date = 03/14/15 Pct Recovery = 69% Analysis Date = 03/03/15 Pct Recovery = 69% Analysis Date = 03/03/15 Pct Recovery = 69% Analysis Date = 02/20/15 Pct Recovery = 69% Analysis Date = 02/20/15 Pct Recovery = 69% Analysis Date = 02/10/15 Pct Recovery = 69% Analysis Date = 02/10/15 Pct Recovery = 69% Analysis Date = 01/30/15 Pct Recovery = 69% Analysis Date = 01/30/15 Pct Recovery = 69% Analysis Date = 01/19/15 Pct Recovery = 69% Analysis Date = 01/19/15 Pct Recovery = 69% Analysis Date = 01/08/15 Pct Recovery = 68% Analysis Date = 01/08/15 Pct Recovery = 68% Analysis Date = 12/28/14 Pct Recovery = 68% Analysis Date = 12/28/14 Pct Recovery = 68% Analysis Date = 12/18/14 Pct Recovery = 68% Analysis Date = 12/18/14 Pct Recovery = 68% Analysis Date = 12/07/14 Pct Recovery = 68% Analysis Date = 12/07/14 Pct Recovery = 68% Analysis Date = 11/26/14 Pct Recovery = 68% Analysis Date = 11/26/14 Pct Recovery = 68% Analysis Date = 11/15/14 Pct Recovery = 68% Analysis Date = 11/15/14 Pct Recovery = 68% Analysis Date = 11/05/14 Pct Recovery = 68% Analysis Date = 11/05/14 Pct Recovery = 68% Analysis Date = 10/25/14 Pct Recovery = 68% Analysis Date = 10/25/14 Pct Recovery = 68% Analysis Date = 10/14/14 Pct Recovery = 67% Analysis Date = 10/14/14 Pct Recovery = 67% Analysis Date = 10/03/14 Pct Recovery = 67% Analysis Date = 10/03/14 Pct Recovery = 67% Analysis Date = 09/23/14 Pct Recovery = 67% Analysis Date = 09/23/14 Pct Recovery = 67% Analysis Date = 09/12/14 Pct Recovery = 67% Analysis Date = 09/12/14 Pct Recovery = 67% Analysis Date = 09/01/14 Pct Recovery = 67% Analysis Date = 09/01/14 Pct Recovery = 67% Analysis Date = 08/21/14 Pct Recovery = 67% Analysis Date = 08/21/14 Pct Recovery = 67% Analysis Date = 08/10/14 Pct Recovery = 67% Analysis Date = 08/10/14 Pct Recovery = 67% Analysis Date = 07/31/14 Pct Recovery = 67% Analysis Date = 07/31/14 Pct Recovery = 67% Analysis Date = 07/20/14 Pct Recovery = 67% Analysis Date = 07/20/14 Pct Recovery = 67% Analysis Date = 07/09/14 Pct Recovery = 67% Analysis Date = 07/09/14 Pct Recovery = 67% Analysis Date = 06/28/14 Pct Recovery = 67% Analysis Date = 06/28/14 Pct Recovery = 67% Analysis Date = 06/18/14 Pct Recovery = 67% Analysis Date = 06/18/14 Pct Recovery = 67% Analysis Date = 06/07/14 Pct Recovery = 67% Analysis Date = 06/07/14 Pct Recovery = 67% Analysis Date = 05/27/14 Pct Recovery = 67% Analysis Date = 05/27/14 Pct Recovery = 67% Analysis Date = 05/16/14 Pct Recovery = 67% Analysis Date = 05/16/14 Pct Recovery = 67% Analysis Date = 05/05/14 Pct Recovery = 66% Analysis Date = 05/05/14 Pct Recovery = 66% Analysis Date = 04/25/14 Pct Recovery = 66% Analysis Date = 04/25/14 Pct Recovery = 66% Analysis Date = 04/14/14 Pct Recovery = 66% Analysis Date = 04/14/14 Pct Recovery = 66% Analysis Date = 04/03/14 Pct Recovery = 66% Analysis Date = 04/03/14 Pct Recovery = 66% Analysis Date = 03/23/14 Pct Recovery = 66% Analysis Date = 03/23/14 Pct Recovery = 66% Analysis Date = 03/13/14 Pct Recovery = 66% Analysis Date = 03/13/14 Pct Recovery = 66% Analysis Date = 03/02/14 Pct Recovery = 66% Analysis Date = 03/02/14 Pct Recovery = 66% Analysis Date = 02/19/14 Pct Recovery = 66% Analysis Date = 02/19/14 Pct Recovery = 66% Analysis Date = 02/08/14 Pct Recovery = 66% Analysis Date = 02/08/14 Pct Recovery = 66% Analysis Date = 01/28/14 Pct Recovery = 66% Analysis Date = 01/28/14 Pct Recovery = 66% Analysis Date = 01/18/14 Pct Recovery = 66% Analysis Date = 01/18/14 Pct Recovery = 66% Analysis Date = 01/07/14 Pct Recovery = 66% Analysis Date = 01/07/14 Pct Recovery = 66% Analysis Date = 12/27/13 Pct Recovery = 66% Analysis Date = 12/27/13 Pct Recovery = 66% Analysis Date = 12/16/13 Pct Recovery = 66% Analysis Date = 12/16/13 Pct Recovery = 66% Analysis Date = 12/06/13 Pct Recovery = 66% Analysis Date = 12/06/13 Pct Recovery = 66% Analysis Date = 11/25/13 Pct Recovery = 65% Analysis Date = 11/25/13 Pct Recovery = 65% Analysis Date = 11/14/13 Pct Recovery = 65% Analysis Date = 11/14/13 Pct Recovery = 65% Analysis Date = 11/03/13 Pct Recovery = 65% Analysis Date = 11/03/13 Pct Recovery = 65% Analysis Date = 10/23/13 Pct Recovery = 65% Analysis Date = 10/23/13 Pct Recovery = 65% Analysis Date = 10/13/13 Pct Recovery = 65% Analysis Date = 10/13/13 Pct Recovery = 65% Analysis Date = 10/02/13 Pct Recovery = 65% Analysis Date = 10/02/13 Pct Recovery = 65% Analysis Date = 09/21/13 Pct Recovery = 65% Analysis Date = 09/21/13 Pct Recovery = 65% Analysis Date = 09/10/13 Pct Recovery = 65% Analysis Date = 09/10/13 Pct Recovery = 65% Analysis Date = 08/31/13 Pct Recovery = 65% Analysis Date = 08/31/13 Pct Recovery = 65% Analysis Date = 08/20/13 Pct Recovery = 65% Analysis Date = 08/20/13 Pct Recovery = 65% Analysis Date = 08/09/13 Pct Recovery = 65% Analysis Date = 08/09/13 Pct Recovery = 65% Analysis Date = 07/29/13 Pct Recovery = 65% Analysis Date = 07/29/13 Pct Recovery = 65% Analysis Date = 07/19/13 Pct Recovery = 65% Analysis Date = 07/19/13 Pct Recovery = 65% Analysis Date = 07/08/13 Pct Recovery = 65% Analysis Date = 07/08/13 Pct Recovery = 65% Analysis Date = 06/27/13 Pct Recovery = 64% Analysis Date = 06/27/13 Pct Recovery = 64% Analysis Date = 06/16/13 Pct Recovery = 64% Analysis Date = 06/16/13 Pct Recovery = 64% Analysis Date = 06/05/13 Pct Recovery = 64% Analysis Date = 06/05/13 Pct Recovery = 64% Analysis Date = 05/26/13 Pct Recovery = 64% Analysis Date = 05/26/13 Pct Recovery = 64% Analysis Date = 05/15/13 Pct Recovery = 64% Analysis Date = 05/15/13 Pct Recovery = 64% Analysis Date = 05/04/13 Pct Recovery = 64% Analysis Date = 05/04/13 Pct Recovery = 64% Analysis Date = 04/23/13 Pct Recovery = 64% Analysis Date = 04/23/13 Pct Recovery = 64% Analysis Date = 04/13/13 Pct Recovery = 64% Analysis Date = 04/13/13 Pct Recovery = 64% Analysis Date = 04/02/13 Pct Recovery = 64% Analysis Date = 04/02/13 Pct Recovery = 64% Analysis Date = 03/22/13 Pct Recovery = 64% Analysis Date = 03/22/13 Pct Recovery = 64% Analysis Date = 03/11/13 Pct Recovery = 63% Analysis Date = 03/11/13 Pct Recovery = 63% Analysis Date = 02/28/13 Pct Recovery = 63% Analysis Date = 02/28/13 Pct Recovery = 63% Analysis Date = 02/18/13 Pct Recovery = 63% Analysis Date = 02/18/13 Pct Recovery = 63% Analysis Date = 02/07/13 Pct Recovery = 63% Analysis Date = 02/07/13 Pct Recovery = 63% Analysis Date = 01/27/13 Pct Recovery = 63% Analysis Date = 01/27/13 Pct Recovery = 63% Analysis Date = 01/16/13 Pct Recovery = 63% Analysis Date = 01/16/13 Pct Recovery = 63% Analysis Date = 01/06/13 Pct Recovery = 63% Analysis Date = 01/06/13 Pct Recovery = 63% Analysis Date = 12/26/12 Pct Recovery = 63% Analysis Date = 12/26/12 Pct Recovery = 63% Analysis Date = 12/15/12 Pct Recovery = 63% Analysis Date = 12/15/12 Pct Recovery = 63% Analysis Date = 12/04/12 Pct Recovery = 62% Analysis Date = 12/04/12 Pct Recovery = 62% Analysis Date = 11/23/12 Pct Recovery = 62% Analysis Date = 11/23/12 Pct Recovery = 62% Analysis Date = 11/13/12 Pct Recovery = 62% Analysis Date = 11/13/12 Pct Recovery = 62% Analysis Date = 11/02/12 Pct Recovery = 62% Analysis Date = 11/02/12 Pct Recovery = 62% Analysis Date = 10/22/12 Pct Recovery = 62% Analysis Date = 10/22/12 Pct Recovery = 62% Analysis Date = 10/11/12 Pct Recovery = 62% Analysis Date = 10/11/12 Pct Recovery = 62% Analysis Date = 10/01/12 Pct Recovery = 62% Analysis Date = 10/01/12 Pct Recovery = 62% Analysis Date = 09/20/12 Pct Recovery = 62% Analysis Date = 09/20/12 Pct Recovery = 62% Analysis Date = 09/09/12 Pct Recovery = 62% Analysis Date = 09/09/12 Pct Recovery = 62% Analysis Date = 08/29/12 Pct Recovery = 62% Analysis Date = 08/29/12 Pct Recovery = 62% Analysis Date = 08/18/12 Pct Recovery = 62% Analysis Date = 08/18/12 Pct Recovery = 62% Analysis Date = 08/08/12 Pct Recovery = 61% Analysis Date = 08/08/12 Pct Recovery = 61% Analysis Date = 07/28/12 Pct Recovery = 61% Analysis Date = 07/28/12 Pct Recovery = 61% Analysis Date = 07/17/12 Pct Recovery = 61% Analysis Date = 07/17/12 Pct Recovery = 61% Analysis Date = 07/06/12 Pct Recovery = 61% Analysis Date = 07/06/12 Pct Recovery = 61% Analysis Date = 06/26/12 Pct Recovery = 61% Analysis Date = 06/26/12 Pct Recovery = 61% Analysis Date = 06/15/12 Pct Recovery = 61% Analysis Date = 06/15/12 Pct Recovery = 61% Analysis Date = 06/04/12 Pct Recovery = 61% Analysis Date = 06/04/12 Pct Recovery = 61% Analysis Date = 05/24/12 Pct Recovery = 61% Analysis Date = 05/24/12 Pct Recovery = 61% Analysis Date = 05/14/12 Pct Recovery = 61% Analysis Date = 05/14/12 Pct Recovery = 61% Analysis Date = 05/03/12 Pct Recovery = 61% Analysis Date = 05/03/12 Pct Recovery = 61% Analysis Date = 04/22/12 Pct Recovery = 61% Analysis Date = 04/22/12 Pct Recovery = 61% Analysis Date = 04/11/12 Pct Recovery = 61% Analysis Date = 04/11/12 Pct Recovery = 61% Analysis Date = 03/31/12 Pct Recovery = 61% Analysis Date = 03/31/12 Pct Recovery = 61% Analysis Date = 03/21/12 Pct Recovery = 61% Analysis Date = 03/21/12 Pct Recovery = 61% Analysis Date = 03/10/12 Pct Recovery = 61% Analysis Date = 03/10/12 Pct Recovery = 61% Analysis Date = 02/28/12 Pct Recovery = 60% Analysis Date = 02/28/12 Pct Recovery = 60% Analysis Date = 02/17/12 Pct Recovery = 60% Analysis Date = 02/17/12 Pct Recovery = 60% Analysis Date = 02/07/12 Pct Recovery = 60% Analysis Date = 02/07/12 Pct Recovery = 60% Analysis Date = 01/27/12 Pct Recovery = 60% Analysis Date = 01/27/12 Pct Recovery = 60% Analysis Date = 01/16/12 Pct Recovery = 60% Analysis Date = 01/16/12 Pct Recovery = 60% Analysis Date = 01/05/12 Pct Recovery = 60% Analysis Date = 01/05/12 Pct Recovery = 60% Analysis Date = 12/25/11 Pct Recovery = 60% Analysis Date = 12/25/11 Pct Recovery = 60% Analysis Date = 12/15/11 Pct Recovery = 60% Analysis Date = 12/15/11 Pct Recovery = 60% Analysis Date = 12/04/11 Pct Recovery = 60% Analysis Date = 12/04/11 Pct Recovery = 60% Analysis Date = 11/23/11 Pct Recovery = 60% Analysis Date = 11/23/11 Pct Recovery = 60% Analysis Date = 11/12/11 Pct Recovery = 60% Analysis Date = 11/12/11 Pct Recovery = 60% Analysis Date = 11/02/11 Pct Recovery = 60% Analysis Date = 11/02/11 Pct Recovery = 60% Analysis Date = 10/22/11 Pct Recovery = 60% Analysis Date = 10/22/11 Pct Recovery = 60% Analysis Date = 10/11/11 Pct Recovery = 60% Analysis Date = 10/11/11 Pct Recovery = 60% Analysis Date = 09/30/11 Pct Recovery = 60% Analysis Date = 09/30/11 Pct Recovery = 60% Analysis Date = 09/19/11 Pct Recovery = 60% Analysis Date = 09/19/11 Pct Recovery = 60% Analysis Date = 09/09/11 Pct Recovery = 59% Analysis Date = 09/09/11 Pct Recovery = 59% Analysis Date = 08/29/11 Pct Recovery = 59% Analysis Date = 08/29/11 Pct Recovery = 59% Analysis Date = 08/18/11 Pct Recovery = 59% Analysis Date = 08/18/11 Pct Recovery = 59% Analysis Date = 08/07/11 Pct Recovery = 59% Analysis Date = 08/07/11 Pct Recovery = 59% Analysis Date = 07/28/11 Pct Recovery = 59% Analysis Date = 07/28/11 Pct Recovery = 59% Analysis Date = 07/17/11 Pct Recovery = 59% Analysis Date = 07/17/11 Pct Recovery = 59% Analysis Date = 07/06/11 Pct Recovery = 59% Analysis Date = 07/06/11 Pct Recovery = 59% Analysis Date = 06/25/11 Pct Recovery = 59% Analysis Date = 06/25/11 Pct Recovery = 59% Analysis Date = 06/14/11 Pct Recovery = 59% Analysis Date = 06/14/11 Pct Recovery = 59% Analysis Date = 06/04/11 Pct Recovery = 59% Analysis Date = 06/04/11 Pct Recovery = 59% Analysis Date = 05/24/11 Pct Recovery = 59% Analysis Date = 05/24/11 Pct Recovery = 59% Analysis Date = 05/13/11 Pct Recovery = 59% Analysis Date = 05/13/11 Pct Recovery = 59% Analysis Date = 05/02/11 Pct Recovery = 59% Analysis Date = 05/02/11 Pct Recovery = 59% Analysis Date = 04/22/11 Pct Recovery = 59% Analysis Date = 04/22/11 Pct Recovery = 59% Analysis Date = 04/11/11 Pct Recovery = 59% Analysis Date = 04/11/11 Pct Recovery = 59% Analysis Date = 03/31/11 Pct Recovery = 59% Analysis Date = 03/31/11 Pct Recovery = 59% Analysis Date = 03/20/11 Pct Recovery = 59% Analysis Date = 03/20/11 Pct Recovery = 59% Analysis Date = 03/10/11 Pct Recovery = 59% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
TRANS-DIETHYLSTILBESTROL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 69 65% 11% 64% 12%
Total 69 65% 11% 64% 12%

Sample Statistics
TRANS-DIETHYLSTILBESTROL

Characteristic N % % Basis
Plotted 69 86% Spiked
Estimated Values 2 3% Spiked
Deleted Values 2 2% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 81 .  
False Negatives 11 14% 11 out of 80
Not Spiked 50 .  
False Positives 0 0% 0 out of 49