BQS OBSP Determination:
1,7-DIMETHYLXANTHINE (P-XANTHINE)
METHOD: 2440 , TESTIDCODE: 67446LCM56
Open Data Set

Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 155% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 148% Analysis Date = 11/24/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 89% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 80 µl & Abs 051315: 80 µl Pct Recovery = 68% Analysis Date = 10/01/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 68% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 80 µl & ERA 0406-15-08: 80 µl Pct Recovery = 85% Analysis Date = 11/05/15 SpikeMix = ERA 0406-15-08: 80 µl & Abs 052215: 80 µl Pct Recovery = 82% Analysis Date = 09/24/16 SpikeMix = Crescent EN160610015: 80 µl & Abs 061416: 80 µl Pct Recovery = 150% Analysis Date = 09/24/16 SpikeMix = Abs 061416: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 140% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 158% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 162% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 173% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 169% Analysis Date = 11/18/16 SpikeMix = ERA 04281604: 80 µl & ERA 04281603: 80 µl Pct Recovery = 149% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & ERA 04281604: 80 µl Pct Recovery = 147% Analysis Date = 04/29/15 SpikeMix = ERA 0319-14-05: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 144% Analysis Date = 03/11/15 SpikeMix = ERA 0318-14-02: 15 µl & Abs 041714: 15 µl Pct Recovery = 141% Analysis Date = 02/06/15 SpikeMix = Abs 041814: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 121% Analysis Date = 12/06/14 SpikeMix = ERA 0318-14-02: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 120% Analysis Date = 10/11/14 SpikeMix = ERA 0318-14-02: 60 µl & ERA 0319-14-04: 60 µl Pct Recovery = 106% Analysis Date = 08/21/14 SpikeMix = ERA 0318-14-02: 60 µl & Abs 041714: 60 µl Pct Recovery = 72% Analysis Date = 07/26/14 SpikeMix = ERA 0319-14-05: 60 µl & ERA 0318-14-02: 60 µl Pct Recovery = 91% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 134% Analysis Date = 12/07/14 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 128% Analysis Date = 10/25/14 SpikeMix = Abs 041614: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 119% Analysis Date = 06/22/14 SpikeMix = Abs 041814: 60 µl & Abs 041614: 60 µl Pct Recovery = 101% Analysis Date = 06/11/14 SpikeMix = Abs 041614: 60 µl & Abs 041714: 60 µl Pct Recovery = 101% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 80% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 69% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-07A: 40 µl & Abs 051315: 40 µl Pct Recovery = 82% Analysis Date = 07/31/15 SpikeMix = Abs 051315: 40 µl & Abs 052215: 40 µl Pct Recovery = 82% Analysis Date = 07/30/15 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 87% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-08: 40 µl & Abs 052215: 40 µl Pct Recovery = 87% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 82% Analysis Date = 11/04/15 SpikeMix = ERA 0406-15-07A: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 75% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-08: 40 µl & ERA 0406-15-09: 40 µl Pct Recovery = 81% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 130% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 130% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 130% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 134% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 102% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 111% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 113% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 117% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 188% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 191% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 170% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 170% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 142% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 154% Analysis Date = 12/07/14 SpikeMix = ERA 0318-14-02: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 135% Analysis Date = 11/04/14 SpikeMix = Abs 041814: 8 µl & ERA 0318-14-02: 8 µl Pct Recovery = 135% Analysis Date = 04/30/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 114% Analysis Date = 02/10/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 116% Analysis Date = 10/24/14 SpikeMix = ERA 0319-14-05: 8 µl & Abs 041614: 8 µl Pct Recovery = 124% Analysis Date = 10/10/14 SpikeMix = Abs 041814: 30 µl & ERA 0318-14-02: 30 µl Pct Recovery = 100% Analysis Date = 08/30/14 SpikeMix = ERA 0318-14-02: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 121% Analysis Date = 07/20/14 SpikeMix = ERA 0318-14-02: 30 µl & Abs 041714: 30 µl Pct Recovery = 71% Analysis Date = 09/12/14 SpikeMix = Abs 041614: 30 µl & ERA 0319-14-04: 30 µl Pct Recovery = 107% Analysis Date = 07/13/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 97% Analysis Date = 05/30/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 93% Analysis Date = 05/17/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 90% Analysis Date = 04/23/14 SpikeMix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.2: 20 µl Pct Recovery = 82% Analysis Date = 02/23/16 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 74% Analysis Date = 08/11/15 SpikeMix = Abs 050115: 20 µl & Abs 051315: 20 µl Pct Recovery = 71% Analysis Date = 06/26/15 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 83% Analysis Date = 06/09/15 SpikeMix = Abs 051315: 20 µl & Abs 050115: 20 µl Pct Recovery = 124% Analysis Date = 04/27/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 113% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 77% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-08: 20 µl & ERA 0406-15-09: 20 µl Pct Recovery = 86% Analysis Date = 11/25/15 SpikeMix = Abs 050115: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 83% Analysis Date = 09/15/15 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 75% Analysis Date = 09/09/15 SpikeMix = ERA 0406-15-08: 20 µl & Abs 052215: 20 µl Pct Recovery = 101% Analysis Date = 04/09/16 SpikeMix = Abs 051315: 10 µl & ERA 0406-15-09: 10 µl Pct Recovery = 79% Analysis Date = 01/04/17 Pct Recovery = 170% Analysis Date = 12/31/16 Pct Recovery = 168% Analysis Date = 12/31/16 Pct Recovery = 168% Analysis Date = 12/26/16 Pct Recovery = 167% Analysis Date = 12/26/16 Pct Recovery = 167% Analysis Date = 12/21/16 Pct Recovery = 166% Analysis Date = 12/21/16 Pct Recovery = 166% Analysis Date = 12/16/16 Pct Recovery = 164% Analysis Date = 12/16/16 Pct Recovery = 164% Analysis Date = 12/11/16 Pct Recovery = 163% Analysis Date = 12/11/16 Pct Recovery = 163% Analysis Date = 12/06/16 Pct Recovery = 162% Analysis Date = 12/06/16 Pct Recovery = 162% Analysis Date = 12/01/16 Pct Recovery = 160% Analysis Date = 12/01/16 Pct Recovery = 160% Analysis Date = 11/26/16 Pct Recovery = 159% Analysis Date = 11/26/16 Pct Recovery = 159% Analysis Date = 11/21/16 Pct Recovery = 158% Analysis Date = 11/21/16 Pct Recovery = 158% Analysis Date = 11/16/16 Pct Recovery = 157% Analysis Date = 11/16/16 Pct Recovery = 157% Analysis Date = 11/11/16 Pct Recovery = 155% Analysis Date = 11/11/16 Pct Recovery = 155% Analysis Date = 11/06/16 Pct Recovery = 154% Analysis Date = 11/06/16 Pct Recovery = 154% Analysis Date = 11/01/16 Pct Recovery = 153% Analysis Date = 11/01/16 Pct Recovery = 153% Analysis Date = 10/27/16 Pct Recovery = 151% Analysis Date = 10/27/16 Pct Recovery = 151% Analysis Date = 10/22/16 Pct Recovery = 150% Analysis Date = 10/22/16 Pct Recovery = 150% Analysis Date = 10/17/16 Pct Recovery = 149% Analysis Date = 10/17/16 Pct Recovery = 149% Analysis Date = 10/13/16 Pct Recovery = 147% Analysis Date = 10/13/16 Pct Recovery = 147% Analysis Date = 10/08/16 Pct Recovery = 146% Analysis Date = 10/08/16 Pct Recovery = 146% Analysis Date = 10/03/16 Pct Recovery = 145% Analysis Date = 10/03/16 Pct Recovery = 145% Analysis Date = 09/28/16 Pct Recovery = 144% Analysis Date = 09/28/16 Pct Recovery = 144% Analysis Date = 09/23/16 Pct Recovery = 142% Analysis Date = 09/23/16 Pct Recovery = 142% Analysis Date = 09/18/16 Pct Recovery = 141% Analysis Date = 09/18/16 Pct Recovery = 141% Analysis Date = 09/13/16 Pct Recovery = 140% Analysis Date = 09/13/16 Pct Recovery = 140% Analysis Date = 09/08/16 Pct Recovery = 138% Analysis Date = 09/08/16 Pct Recovery = 138% Analysis Date = 09/03/16 Pct Recovery = 137% Analysis Date = 09/03/16 Pct Recovery = 137% Analysis Date = 08/29/16 Pct Recovery = 136% Analysis Date = 08/29/16 Pct Recovery = 136% Analysis Date = 08/24/16 Pct Recovery = 134% Analysis Date = 08/24/16 Pct Recovery = 134% Analysis Date = 08/19/16 Pct Recovery = 133% Analysis Date = 08/19/16 Pct Recovery = 133% Analysis Date = 08/14/16 Pct Recovery = 132% Analysis Date = 08/14/16 Pct Recovery = 132% Analysis Date = 08/09/16 Pct Recovery = 130% Analysis Date = 08/09/16 Pct Recovery = 130% Analysis Date = 08/04/16 Pct Recovery = 129% Analysis Date = 08/04/16 Pct Recovery = 129% Analysis Date = 07/30/16 Pct Recovery = 128% Analysis Date = 07/30/16 Pct Recovery = 128% Analysis Date = 07/25/16 Pct Recovery = 127% Analysis Date = 07/25/16 Pct Recovery = 127% Analysis Date = 07/21/16 Pct Recovery = 125% Analysis Date = 07/21/16 Pct Recovery = 125% Analysis Date = 07/16/16 Pct Recovery = 124% Analysis Date = 07/16/16 Pct Recovery = 124% Analysis Date = 07/11/16 Pct Recovery = 123% Analysis Date = 07/11/16 Pct Recovery = 123% Analysis Date = 07/06/16 Pct Recovery = 122% Analysis Date = 07/06/16 Pct Recovery = 122% Analysis Date = 07/01/16 Pct Recovery = 121% Analysis Date = 07/01/16 Pct Recovery = 121% Analysis Date = 06/26/16 Pct Recovery = 120% Analysis Date = 06/26/16 Pct Recovery = 120% Analysis Date = 06/21/16 Pct Recovery = 118% Analysis Date = 06/21/16 Pct Recovery = 118% Analysis Date = 06/16/16 Pct Recovery = 117% Analysis Date = 06/16/16 Pct Recovery = 117% Analysis Date = 06/11/16 Pct Recovery = 116% Analysis Date = 06/11/16 Pct Recovery = 116% Analysis Date = 06/06/16 Pct Recovery = 115% Analysis Date = 06/06/16 Pct Recovery = 115% Analysis Date = 06/01/16 Pct Recovery = 114% Analysis Date = 06/01/16 Pct Recovery = 114% Analysis Date = 05/27/16 Pct Recovery = 113% Analysis Date = 05/27/16 Pct Recovery = 113% Analysis Date = 05/22/16 Pct Recovery = 112% Analysis Date = 05/22/16 Pct Recovery = 112% Analysis Date = 05/17/16 Pct Recovery = 111% Analysis Date = 05/17/16 Pct Recovery = 111% Analysis Date = 05/12/16 Pct Recovery = 109% Analysis Date = 05/12/16 Pct Recovery = 109% Analysis Date = 05/07/16 Pct Recovery = 108% Analysis Date = 05/07/16 Pct Recovery = 108% Analysis Date = 05/02/16 Pct Recovery = 107% Analysis Date = 05/02/16 Pct Recovery = 107% Analysis Date = 04/28/16 Pct Recovery = 106% Analysis Date = 04/28/16 Pct Recovery = 106% Analysis Date = 04/23/16 Pct Recovery = 105% Analysis Date = 04/23/16 Pct Recovery = 105% Analysis Date = 04/18/16 Pct Recovery = 104% Analysis Date = 04/18/16 Pct Recovery = 104% Analysis Date = 04/13/16 Pct Recovery = 103% Analysis Date = 04/13/16 Pct Recovery = 103% Analysis Date = 04/08/16 Pct Recovery = 102% Analysis Date = 04/08/16 Pct Recovery = 102% Analysis Date = 04/03/16 Pct Recovery = 101% Analysis Date = 04/03/16 Pct Recovery = 101% Analysis Date = 03/29/16 Pct Recovery = 100% Analysis Date = 03/29/16 Pct Recovery = 100% Analysis Date = 03/24/16 Pct Recovery = 99% Analysis Date = 03/24/16 Pct Recovery = 99% Analysis Date = 03/19/16 Pct Recovery = 98% Analysis Date = 03/19/16 Pct Recovery = 98% Analysis Date = 03/14/16 Pct Recovery = 98% Analysis Date = 03/14/16 Pct Recovery = 98% Analysis Date = 03/09/16 Pct Recovery = 97% Analysis Date = 03/09/16 Pct Recovery = 97% Analysis Date = 03/04/16 Pct Recovery = 96% Analysis Date = 03/04/16 Pct Recovery = 96% Analysis Date = 02/28/16 Pct Recovery = 95% Analysis Date = 02/28/16 Pct Recovery = 95% Analysis Date = 02/23/16 Pct Recovery = 94% Analysis Date = 02/23/16 Pct Recovery = 94% Analysis Date = 02/18/16 Pct Recovery = 94% Analysis Date = 02/18/16 Pct Recovery = 94% Analysis Date = 02/13/16 Pct Recovery = 94% Analysis Date = 02/13/16 Pct Recovery = 94% Analysis Date = 02/09/16 Pct Recovery = 93% Analysis Date = 02/09/16 Pct Recovery = 93% Analysis Date = 02/04/16 Pct Recovery = 93% Analysis Date = 02/04/16 Pct Recovery = 93% Analysis Date = 01/30/16 Pct Recovery = 93% Analysis Date = 01/30/16 Pct Recovery = 93% Analysis Date = 01/25/16 Pct Recovery = 93% Analysis Date = 01/25/16 Pct Recovery = 93% Analysis Date = 01/20/16 Pct Recovery = 92% Analysis Date = 01/20/16 Pct Recovery = 92% Analysis Date = 01/15/16 Pct Recovery = 92% Analysis Date = 01/15/16 Pct Recovery = 92% Analysis Date = 01/10/16 Pct Recovery = 92% Analysis Date = 01/10/16 Pct Recovery = 92% Analysis Date = 01/05/16 Pct Recovery = 91% Analysis Date = 01/05/16 Pct Recovery = 91% Analysis Date = 12/31/15 Pct Recovery = 91% Analysis Date = 12/31/15 Pct Recovery = 91% Analysis Date = 12/26/15 Pct Recovery = 91% Analysis Date = 12/26/15 Pct Recovery = 91% Analysis Date = 12/21/15 Pct Recovery = 91% Analysis Date = 12/21/15 Pct Recovery = 91% Analysis Date = 12/16/15 Pct Recovery = 90% Analysis Date = 12/16/15 Pct Recovery = 90% Analysis Date = 12/11/15 Pct Recovery = 90% Analysis Date = 12/11/15 Pct Recovery = 90% Analysis Date = 12/06/15 Pct Recovery = 90% Analysis Date = 12/06/15 Pct Recovery = 90% Analysis Date = 12/01/15 Pct Recovery = 89% Analysis Date = 12/01/15 Pct Recovery = 89% Analysis Date = 11/26/15 Pct Recovery = 89% Analysis Date = 11/26/15 Pct Recovery = 89% Analysis Date = 11/21/15 Pct Recovery = 89% Analysis Date = 11/21/15 Pct Recovery = 89% Analysis Date = 11/17/15 Pct Recovery = 88% Analysis Date = 11/17/15 Pct Recovery = 88% Analysis Date = 11/12/15 Pct Recovery = 88% Analysis Date = 11/12/15 Pct Recovery = 88% Analysis Date = 11/07/15 Pct Recovery = 88% Analysis Date = 11/07/15 Pct Recovery = 88% Analysis Date = 11/02/15 Pct Recovery = 88% Analysis Date = 11/02/15 Pct Recovery = 88% Analysis Date = 10/28/15 Pct Recovery = 88% Analysis Date = 10/28/15 Pct Recovery = 88% Analysis Date = 10/23/15 Pct Recovery = 89% Analysis Date = 10/23/15 Pct Recovery = 89% Analysis Date = 10/18/15 Pct Recovery = 89% Analysis Date = 10/18/15 Pct Recovery = 89% Analysis Date = 10/13/15 Pct Recovery = 90% Analysis Date = 10/13/15 Pct Recovery = 90% Analysis Date = 10/08/15 Pct Recovery = 90% Analysis Date = 10/08/15 Pct Recovery = 90% Analysis Date = 10/03/15 Pct Recovery = 91% Analysis Date = 10/03/15 Pct Recovery = 91% Analysis Date = 09/28/15 Pct Recovery = 91% Analysis Date = 09/28/15 Pct Recovery = 91% Analysis Date = 09/23/15 Pct Recovery = 92% Analysis Date = 09/23/15 Pct Recovery = 92% Analysis Date = 09/18/15 Pct Recovery = 92% Analysis Date = 09/18/15 Pct Recovery = 92% Analysis Date = 09/13/15 Pct Recovery = 93% Analysis Date = 09/13/15 Pct Recovery = 93% Analysis Date = 09/08/15 Pct Recovery = 93% Analysis Date = 09/08/15 Pct Recovery = 93% Analysis Date = 09/03/15 Pct Recovery = 94% Analysis Date = 09/03/15 Pct Recovery = 94% Analysis Date = 08/29/15 Pct Recovery = 94% Analysis Date = 08/29/15 Pct Recovery = 94% Analysis Date = 08/25/15 Pct Recovery = 95% Analysis Date = 08/25/15 Pct Recovery = 95% Analysis Date = 08/20/15 Pct Recovery = 95% Analysis Date = 08/20/15 Pct Recovery = 95% Analysis Date = 08/15/15 Pct Recovery = 96% Analysis Date = 08/15/15 Pct Recovery = 96% Analysis Date = 08/10/15 Pct Recovery = 96% Analysis Date = 08/10/15 Pct Recovery = 96% Analysis Date = 08/05/15 Pct Recovery = 97% Analysis Date = 08/05/15 Pct Recovery = 97% Analysis Date = 07/31/15 Pct Recovery = 97% Analysis Date = 07/31/15 Pct Recovery = 97% Analysis Date = 07/26/15 Pct Recovery = 98% Analysis Date = 07/26/15 Pct Recovery = 98% Analysis Date = 07/21/15 Pct Recovery = 98% Analysis Date = 07/21/15 Pct Recovery = 98% Analysis Date = 07/16/15 Pct Recovery = 98% Analysis Date = 07/16/15 Pct Recovery = 98% Analysis Date = 07/11/15 Pct Recovery = 99% Analysis Date = 07/11/15 Pct Recovery = 99% Analysis Date = 07/06/15 Pct Recovery = 99% Analysis Date = 07/06/15 Pct Recovery = 99% Analysis Date = 07/01/15 Pct Recovery = 100% Analysis Date = 07/01/15 Pct Recovery = 100% Analysis Date = 06/26/15 Pct Recovery = 100% Analysis Date = 06/26/15 Pct Recovery = 100% Analysis Date = 06/21/15 Pct Recovery = 100% Analysis Date = 06/21/15 Pct Recovery = 100% Analysis Date = 06/16/15 Pct Recovery = 101% Analysis Date = 06/16/15 Pct Recovery = 101% Analysis Date = 06/11/15 Pct Recovery = 101% Analysis Date = 06/11/15 Pct Recovery = 101% Analysis Date = 06/07/15 Pct Recovery = 102% Analysis Date = 06/07/15 Pct Recovery = 102% Analysis Date = 06/02/15 Pct Recovery = 102% Analysis Date = 06/02/15 Pct Recovery = 102% Analysis Date = 05/28/15 Pct Recovery = 102% Analysis Date = 05/28/15 Pct Recovery = 102% Analysis Date = 05/23/15 Pct Recovery = 103% Analysis Date = 05/23/15 Pct Recovery = 103% Analysis Date = 05/18/15 Pct Recovery = 103% Analysis Date = 05/18/15 Pct Recovery = 103% Analysis Date = 05/13/15 Pct Recovery = 104% Analysis Date = 05/13/15 Pct Recovery = 104% Analysis Date = 05/08/15 Pct Recovery = 104% Analysis Date = 05/08/15 Pct Recovery = 104% Analysis Date = 05/03/15 Pct Recovery = 104% Analysis Date = 05/03/15 Pct Recovery = 104% Analysis Date = 04/28/15 Pct Recovery = 105% Analysis Date = 04/28/15 Pct Recovery = 105% Analysis Date = 04/23/15 Pct Recovery = 105% Analysis Date = 04/23/15 Pct Recovery = 105% Analysis Date = 04/18/15 Pct Recovery = 105% Analysis Date = 04/18/15 Pct Recovery = 105% Analysis Date = 04/13/15 Pct Recovery = 105% Analysis Date = 04/13/15 Pct Recovery = 105% Analysis Date = 04/08/15 Pct Recovery = 105% Analysis Date = 04/08/15 Pct Recovery = 105% Analysis Date = 04/03/15 Pct Recovery = 105% Analysis Date = 04/03/15 Pct Recovery = 105% Analysis Date = 03/29/15 Pct Recovery = 105% Analysis Date = 03/29/15 Pct Recovery = 105% Analysis Date = 03/24/15 Pct Recovery = 105% Analysis Date = 03/24/15 Pct Recovery = 105% Analysis Date = 03/19/15 Pct Recovery = 105% Analysis Date = 03/19/15 Pct Recovery = 105% Analysis Date = 03/15/15 Pct Recovery = 105% Analysis Date = 03/15/15 Pct Recovery = 105% Analysis Date = 03/10/15 Pct Recovery = 105% Analysis Date = 03/10/15 Pct Recovery = 105% Analysis Date = 03/05/15 Pct Recovery = 105% Analysis Date = 03/05/15 Pct Recovery = 105% Analysis Date = 02/28/15 Pct Recovery = 105% Analysis Date = 02/28/15 Pct Recovery = 105% Analysis Date = 02/23/15 Pct Recovery = 106% Analysis Date = 02/23/15 Pct Recovery = 106% Analysis Date = 02/18/15 Pct Recovery = 106% Analysis Date = 02/18/15 Pct Recovery = 106% Analysis Date = 02/13/15 Pct Recovery = 106% Analysis Date = 02/13/15 Pct Recovery = 106% Analysis Date = 02/08/15 Pct Recovery = 106% Analysis Date = 02/08/15 Pct Recovery = 106% Analysis Date = 02/03/15 Pct Recovery = 106% Analysis Date = 02/03/15 Pct Recovery = 106% Analysis Date = 01/29/15 Pct Recovery = 106% Analysis Date = 01/29/15 Pct Recovery = 106% Analysis Date = 01/24/15 Pct Recovery = 106% Analysis Date = 01/24/15 Pct Recovery = 106% Analysis Date = 01/19/15 Pct Recovery = 106% Analysis Date = 01/19/15 Pct Recovery = 106% Analysis Date = 01/14/15 Pct Recovery = 106% Analysis Date = 01/14/15 Pct Recovery = 106% Analysis Date = 01/09/15 Pct Recovery = 106% Analysis Date = 01/09/15 Pct Recovery = 106% Analysis Date = 01/04/15 Pct Recovery = 106% Analysis Date = 01/04/15 Pct Recovery = 106% Analysis Date = 12/30/14 Pct Recovery = 106% Analysis Date = 12/30/14 Pct Recovery = 106% Analysis Date = 12/25/14 Pct Recovery = 106% Analysis Date = 12/25/14 Pct Recovery = 106% Analysis Date = 12/21/14 Pct Recovery = 106% Analysis Date = 12/21/14 Pct Recovery = 106% Analysis Date = 12/16/14 Pct Recovery = 106% Analysis Date = 12/16/14 Pct Recovery = 106% Analysis Date = 12/11/14 Pct Recovery = 106% Analysis Date = 12/11/14 Pct Recovery = 106% Analysis Date = 12/06/14 Pct Recovery = 107% Analysis Date = 12/06/14 Pct Recovery = 107% Analysis Date = 12/01/14 Pct Recovery = 106% Analysis Date = 12/01/14 Pct Recovery = 106% Analysis Date = 11/26/14 Pct Recovery = 106% Analysis Date = 11/26/14 Pct Recovery = 106% Analysis Date = 11/21/14 Pct Recovery = 106% Analysis Date = 11/21/14 Pct Recovery = 106% Analysis Date = 11/16/14 Pct Recovery = 106% Analysis Date = 11/16/14 Pct Recovery = 106% Analysis Date = 11/11/14 Pct Recovery = 106% Analysis Date = 11/11/14 Pct Recovery = 106% Analysis Date = 11/06/14 Pct Recovery = 106% Analysis Date = 11/06/14 Pct Recovery = 106% Analysis Date = 11/01/14 Pct Recovery = 106% Analysis Date = 11/01/14 Pct Recovery = 106% Analysis Date = 10/27/14 Pct Recovery = 106% Analysis Date = 10/27/14 Pct Recovery = 106% Analysis Date = 10/22/14 Pct Recovery = 106% Analysis Date = 10/22/14 Pct Recovery = 106% Analysis Date = 10/17/14 Pct Recovery = 106% Analysis Date = 10/17/14 Pct Recovery = 106% Analysis Date = 10/12/14 Pct Recovery = 106% Analysis Date = 10/12/14 Pct Recovery = 106% Analysis Date = 10/07/14 Pct Recovery = 106% Analysis Date = 10/07/14 Pct Recovery = 106% Analysis Date = 10/03/14 Pct Recovery = 106% Analysis Date = 10/03/14 Pct Recovery = 106% Analysis Date = 09/28/14 Pct Recovery = 106% Analysis Date = 09/28/14 Pct Recovery = 106% Analysis Date = 09/23/14 Pct Recovery = 105% Analysis Date = 09/23/14 Pct Recovery = 105% Analysis Date = 09/18/14 Pct Recovery = 105% Analysis Date = 09/18/14 Pct Recovery = 105% Analysis Date = 09/13/14 Pct Recovery = 105% Analysis Date = 09/13/14 Pct Recovery = 105% Analysis Date = 09/08/14 Pct Recovery = 105% Analysis Date = 09/08/14 Pct Recovery = 105% Analysis Date = 09/03/14 Pct Recovery = 105% Analysis Date = 09/03/14 Pct Recovery = 105% Analysis Date = 08/29/14 Pct Recovery = 105% Analysis Date = 08/29/14 Pct Recovery = 105% Analysis Date = 08/24/14 Pct Recovery = 105% Analysis Date = 08/24/14 Pct Recovery = 105% Analysis Date = 08/19/14 Pct Recovery = 105% Analysis Date = 08/19/14 Pct Recovery = 105% Analysis Date = 08/14/14 Pct Recovery = 104% Analysis Date = 08/14/14 Pct Recovery = 104% Analysis Date = 08/09/14 Pct Recovery = 104% Analysis Date = 08/09/14 Pct Recovery = 104% Analysis Date = 08/04/14 Pct Recovery = 104% Analysis Date = 08/04/14 Pct Recovery = 104% Analysis Date = 07/30/14 Pct Recovery = 104% Analysis Date = 07/30/14 Pct Recovery = 104% Analysis Date = 07/25/14 Pct Recovery = 104% Analysis Date = 07/25/14 Pct Recovery = 104% Analysis Date = 07/20/14 Pct Recovery = 104% Analysis Date = 07/20/14 Pct Recovery = 104% Analysis Date = 07/15/14 Pct Recovery = 103% Analysis Date = 07/15/14 Pct Recovery = 103% Analysis Date = 07/11/14 Pct Recovery = 103% Analysis Date = 07/11/14 Pct Recovery = 103% Analysis Date = 07/06/14 Pct Recovery = 103% Analysis Date = 07/06/14 Pct Recovery = 103% Analysis Date = 07/01/14 Pct Recovery = 103% Analysis Date = 07/01/14 Pct Recovery = 103% Analysis Date = 06/26/14 Pct Recovery = 103% Analysis Date = 06/26/14 Pct Recovery = 103% Analysis Date = 06/21/14 Pct Recovery = 103% Analysis Date = 06/21/14 Pct Recovery = 103% Analysis Date = 06/16/14 Pct Recovery = 102% Analysis Date = 06/16/14 Pct Recovery = 102% Analysis Date = 06/11/14 Pct Recovery = 102% Analysis Date = 06/11/14 Pct Recovery = 102% Analysis Date = 06/06/14 Pct Recovery = 102% Analysis Date = 06/06/14 Pct Recovery = 102% Analysis Date = 06/01/14 Pct Recovery = 102% Analysis Date = 06/01/14 Pct Recovery = 102% Analysis Date = 05/27/14 Pct Recovery = 101% Analysis Date = 05/27/14 Pct Recovery = 101% Analysis Date = 05/22/14 Pct Recovery = 101% Analysis Date = 05/22/14 Pct Recovery = 101% Analysis Date = 05/17/14 Pct Recovery = 101% Analysis Date = 05/17/14 Pct Recovery = 101% Analysis Date = 05/12/14 Pct Recovery = 101% Analysis Date = 05/12/14 Pct Recovery = 101% Analysis Date = 05/07/14 Pct Recovery = 100% Analysis Date = 05/07/14 Pct Recovery = 100% Analysis Date = 05/02/14 Pct Recovery = 100% Analysis Date = 05/02/14 Pct Recovery = 100% Analysis Date = 04/27/14 Pct Recovery = 100% Analysis Date = 04/27/14 Pct Recovery = 100% Analysis Date = 04/23/14 Pct Recovery = 100% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
1,7-DIMETHYLXANTHINE (P-XANTHINE)

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 1 79% . 79% 0%
>= Reporting Level 73 114% 33% 113% 38%
Total 74 113% 33% 112% 39%

Sample Statistics
1,7-DIMETHYLXANTHINE (P-XANTHINE)

Characteristic N % % Basis
Plotted 74 97% Spiked
Estimated Values 27 36% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 1 1% Spiked
Spiked 76 .  
False Negatives 1 1% 1 out of 76
Not Spiked 39 .  
False Positives 0 0% 0 out of 39

BQS OBSP Determination:
10-HYDROXY-AMITRIPTYLINE
METHOD: 2440 , TESTIDCODE: 67995LCM56
Open Data Set

Analysis Date = 01/17/16 SpikeMix = ERA 0406-15-09: 80 µl & ERA 0406-15-07A: 80 µl Pct Recovery = 91% Analysis Date = 11/24/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 96% Analysis Date = 11/05/15 SpikeMix = ERA 0406-15-08: 80 µl & Abs 052215: 80 µl Pct Recovery = 75% Analysis Date = 11/04/15 SpikeMix = Abs 052215: 80 µl & Abs 050115: 80 µl Pct Recovery = 68% Analysis Date = 10/01/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 150% Analysis Date = 09/24/16 SpikeMix = Crescent EN160610015: 80 µl & Abs 061416: 80 µl Pct Recovery = 91% Analysis Date = 09/24/16 SpikeMix = Abs 061416: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 92% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 86% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 88% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 83% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 84% Analysis Date = 05/07/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 54% Analysis Date = 03/11/15 SpikeMix = ERA 0318-14-02: 15 µl & Abs 041714: 15 µl Pct Recovery = 49% Analysis Date = 01/16/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 43% Analysis Date = 12/06/14 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 32% Analysis Date = 08/21/14 SpikeMix = ERA 0318-14-02: 60 µl & Abs 041714: 60 µl Pct Recovery = 43% Analysis Date = 07/12/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 59% Analysis Date = 06/11/14 SpikeMix = Abs 041614: 60 µl & Abs 041714: 60 µl Pct Recovery = 51% Analysis Date = 05/21/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 60% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-08: 40 µl & Abs 052215: 40 µl Pct Recovery = 67% Analysis Date = 02/23/16 SpikeMix = Abs 052215: 40 µl & Abs 050115: 40 µl Pct Recovery = 70% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-08: 40 µl & ERA 0406-15-09: 40 µl Pct Recovery = 82% Analysis Date = 09/10/15 SpikeMix = Abs 052215: 40 µl & ERA 0406-15-07A: 40 µl Pct Recovery = 62% Analysis Date = 07/31/15 SpikeMix = ERA 0406-15-09: 40 µl & Abs 050115: 40 µl Pct Recovery = 84% Analysis Date = 07/31/15 SpikeMix = Abs 051315: 40 µl & Abs 052215: 40 µl Pct Recovery = 62% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 66% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 70% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 58% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 70% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 53% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 65% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 53% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 60% Analysis Date = 11/04/14 SpikeMix = Abs 041714: 8 µl & ERA 0319-14-05: 8 µl Pct Recovery = 34% Analysis Date = 10/10/14 SpikeMix = Abs 041714: 30 µl & Abs 041814: 30 µl Pct Recovery = 30% Analysis Date = 07/20/14 SpikeMix = ERA 0318-14-02: 30 µl & Abs 041714: 30 µl Pct Recovery = 36% Analysis Date = 06/28/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 61% Analysis Date = 05/17/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 72% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 69% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 53% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 92% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 61% Analysis Date = 02/23/16 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 70% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-08: 20 µl & ERA 0406-15-09: 20 µl Pct Recovery = 83% Analysis Date = 11/24/15 SpikeMix = ERA 0406-15-09: 20 µl & Abs 050115: 20 µl Pct Recovery = 99% Analysis Date = 11/24/15 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 71% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-09: 20 µl Pct Recovery = 114% Analysis Date = 09/09/15 SpikeMix = ERA 0406-15-08: 20 µl & Abs 052215: 20 µl Pct Recovery = 66% Analysis Date = 08/27/15 SpikeMix = Abs 052215: 20 µl & Abs 050115: 20 µl Pct Recovery = 82% Analysis Date = 07/09/15 SpikeMix = Abs 050115: 20 µl & Abs 052215: 20 µl Pct Recovery = 47% Analysis Date = 06/26/15 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 51% Analysis Date = 04/09/16 SpikeMix = Abs 051315: 10 µl & ERA 0406-15-09: 10 µl Pct Recovery = 56% Analysis Date = 04/09/16 SpikeMix = Abs 051315: 10 µl & ERA 0406-15-09: 10 µl Pct Recovery = 99% Analysis Date = 12/16/16 Pct Recovery = 71% Analysis Date = 12/11/16 Pct Recovery = 71% Analysis Date = 12/11/16 Pct Recovery = 71% Analysis Date = 12/06/16 Pct Recovery = 71% Analysis Date = 12/06/16 Pct Recovery = 71% Analysis Date = 12/01/16 Pct Recovery = 71% Analysis Date = 12/01/16 Pct Recovery = 71% Analysis Date = 11/27/16 Pct Recovery = 71% Analysis Date = 11/27/16 Pct Recovery = 71% Analysis Date = 11/22/16 Pct Recovery = 71% Analysis Date = 11/22/16 Pct Recovery = 71% Analysis Date = 11/17/16 Pct Recovery = 71% Analysis Date = 11/17/16 Pct Recovery = 71% Analysis Date = 11/12/16 Pct Recovery = 71% Analysis Date = 11/12/16 Pct Recovery = 71% Analysis Date = 11/08/16 Pct Recovery = 71% Analysis Date = 11/08/16 Pct Recovery = 71% Analysis Date = 11/03/16 Pct Recovery = 71% Analysis Date = 11/03/16 Pct Recovery = 71% Analysis Date = 10/29/16 Pct Recovery = 71% Analysis Date = 10/29/16 Pct Recovery = 71% Analysis Date = 10/25/16 Pct Recovery = 71% Analysis Date = 10/25/16 Pct Recovery = 71% Analysis Date = 10/20/16 Pct Recovery = 71% Analysis Date = 10/20/16 Pct Recovery = 71% Analysis Date = 10/15/16 Pct Recovery = 72% Analysis Date = 10/15/16 Pct Recovery = 72% Analysis Date = 10/10/16 Pct Recovery = 72% Analysis Date = 10/10/16 Pct Recovery = 72% Analysis Date = 10/06/16 Pct Recovery = 72% Analysis Date = 10/06/16 Pct Recovery = 72% Analysis Date = 10/01/16 Pct Recovery = 72% Analysis Date = 10/01/16 Pct Recovery = 72% Analysis Date = 09/26/16 Pct Recovery = 72% Analysis Date = 09/26/16 Pct Recovery = 72% Analysis Date = 09/22/16 Pct Recovery = 72% Analysis Date = 09/22/16 Pct Recovery = 72% Analysis Date = 09/17/16 Pct Recovery = 72% Analysis Date = 09/17/16 Pct Recovery = 72% Analysis Date = 09/12/16 Pct Recovery = 72% Analysis Date = 09/12/16 Pct Recovery = 72% Analysis Date = 09/07/16 Pct Recovery = 72% Analysis Date = 09/07/16 Pct Recovery = 72% Analysis Date = 09/03/16 Pct Recovery = 72% Analysis Date = 09/03/16 Pct Recovery = 72% Analysis Date = 08/29/16 Pct Recovery = 72% Analysis Date = 08/29/16 Pct Recovery = 72% Analysis Date = 08/24/16 Pct Recovery = 72% Analysis Date = 08/24/16 Pct Recovery = 72% Analysis Date = 08/20/16 Pct Recovery = 72% Analysis Date = 08/20/16 Pct Recovery = 72% Analysis Date = 08/15/16 Pct Recovery = 72% Analysis Date = 08/15/16 Pct Recovery = 72% Analysis Date = 08/10/16 Pct Recovery = 72% Analysis Date = 08/10/16 Pct Recovery = 72% Analysis Date = 08/05/16 Pct Recovery = 72% Analysis Date = 08/05/16 Pct Recovery = 72% Analysis Date = 08/01/16 Pct Recovery = 73% Analysis Date = 08/01/16 Pct Recovery = 73% Analysis Date = 07/27/16 Pct Recovery = 73% Analysis Date = 07/27/16 Pct Recovery = 73% Analysis Date = 07/22/16 Pct Recovery = 73% Analysis Date = 07/22/16 Pct Recovery = 73% Analysis Date = 07/17/16 Pct Recovery = 73% Analysis Date = 07/17/16 Pct Recovery = 73% Analysis Date = 07/13/16 Pct Recovery = 73% Analysis Date = 07/13/16 Pct Recovery = 73% Analysis Date = 07/08/16 Pct Recovery = 73% Analysis Date = 07/08/16 Pct Recovery = 73% Analysis Date = 07/03/16 Pct Recovery = 73% Analysis Date = 07/03/16 Pct Recovery = 73% Analysis Date = 06/29/16 Pct Recovery = 73% Analysis Date = 06/29/16 Pct Recovery = 73% Analysis Date = 06/24/16 Pct Recovery = 73% Analysis Date = 06/24/16 Pct Recovery = 73% Analysis Date = 06/19/16 Pct Recovery = 74% Analysis Date = 06/19/16 Pct Recovery = 74% Analysis Date = 06/14/16 Pct Recovery = 74% Analysis Date = 06/14/16 Pct Recovery = 74% Analysis Date = 06/10/16 Pct Recovery = 74% Analysis Date = 06/10/16 Pct Recovery = 74% Analysis Date = 06/05/16 Pct Recovery = 74% Analysis Date = 06/05/16 Pct Recovery = 74% Analysis Date = 05/31/16 Pct Recovery = 74% Analysis Date = 05/31/16 Pct Recovery = 74% Analysis Date = 05/27/16 Pct Recovery = 74% Analysis Date = 05/27/16 Pct Recovery = 74% Analysis Date = 05/22/16 Pct Recovery = 74% Analysis Date = 05/22/16 Pct Recovery = 74% Analysis Date = 05/17/16 Pct Recovery = 75% Analysis Date = 05/17/16 Pct Recovery = 75% Analysis Date = 05/12/16 Pct Recovery = 75% Analysis Date = 05/12/16 Pct Recovery = 75% Analysis Date = 05/08/16 Pct Recovery = 75% Analysis Date = 05/08/16 Pct Recovery = 75% Analysis Date = 05/03/16 Pct Recovery = 75% Analysis Date = 05/03/16 Pct Recovery = 75% Analysis Date = 04/28/16 Pct Recovery = 75% Analysis Date = 04/28/16 Pct Recovery = 75% Analysis Date = 04/24/16 Pct Recovery = 75% Analysis Date = 04/24/16 Pct Recovery = 75% Analysis Date = 04/19/16 Pct Recovery = 75% Analysis Date = 04/19/16 Pct Recovery = 75% Analysis Date = 04/14/16 Pct Recovery = 75% Analysis Date = 04/14/16 Pct Recovery = 75% Analysis Date = 04/09/16 Pct Recovery = 76% Analysis Date = 04/09/16 Pct Recovery = 76% Analysis Date = 04/05/16 Pct Recovery = 76% Analysis Date = 04/05/16 Pct Recovery = 76% Analysis Date = 03/31/16 Pct Recovery = 76% Analysis Date = 03/31/16 Pct Recovery = 76% Analysis Date = 03/26/16 Pct Recovery = 76% Analysis Date = 03/26/16 Pct Recovery = 76% Analysis Date = 03/21/16 Pct Recovery = 76% Analysis Date = 03/21/16 Pct Recovery = 76% Analysis Date = 03/17/16 Pct Recovery = 76% Analysis Date = 03/17/16 Pct Recovery = 76% Analysis Date = 03/12/16 Pct Recovery = 76% Analysis Date = 03/12/16 Pct Recovery = 76% Analysis Date = 03/07/16 Pct Recovery = 77% Analysis Date = 03/07/16 Pct Recovery = 77% Analysis Date = 03/03/16 Pct Recovery = 77% Analysis Date = 03/03/16 Pct Recovery = 77% Analysis Date = 02/27/16 Pct Recovery = 77% Analysis Date = 02/27/16 Pct Recovery = 77% Analysis Date = 02/22/16 Pct Recovery = 78% Analysis Date = 02/22/16 Pct Recovery = 78% Analysis Date = 02/17/16 Pct Recovery = 78% Analysis Date = 02/17/16 Pct Recovery = 78% Analysis Date = 02/13/16 Pct Recovery = 78% Analysis Date = 02/13/16 Pct Recovery = 78% Analysis Date = 02/08/16 Pct Recovery = 78% Analysis Date = 02/08/16 Pct Recovery = 78% Analysis Date = 02/03/16 Pct Recovery = 78% Analysis Date = 02/03/16 Pct Recovery = 78% Analysis Date = 01/30/16 Pct Recovery = 78% Analysis Date = 01/30/16 Pct Recovery = 78% Analysis Date = 01/25/16 Pct Recovery = 78% Analysis Date = 01/25/16 Pct Recovery = 78% Analysis Date = 01/20/16 Pct Recovery = 79% Analysis Date = 01/20/16 Pct Recovery = 79% Analysis Date = 01/15/16 Pct Recovery = 79% Analysis Date = 01/15/16 Pct Recovery = 79% Analysis Date = 01/11/16 Pct Recovery = 79% Analysis Date = 01/11/16 Pct Recovery = 79% Analysis Date = 01/06/16 Pct Recovery = 79% Analysis Date = 01/06/16 Pct Recovery = 79% Analysis Date = 01/01/16 Pct Recovery = 79% Analysis Date = 01/01/16 Pct Recovery = 79% Analysis Date = 12/28/15 Pct Recovery = 79% Analysis Date = 12/28/15 Pct Recovery = 79% Analysis Date = 12/23/15 Pct Recovery = 79% Analysis Date = 12/23/15 Pct Recovery = 79% Analysis Date = 12/18/15 Pct Recovery = 79% Analysis Date = 12/18/15 Pct Recovery = 79% Analysis Date = 12/13/15 Pct Recovery = 80% Analysis Date = 12/13/15 Pct Recovery = 80% Analysis Date = 12/09/15 Pct Recovery = 80% Analysis Date = 12/09/15 Pct Recovery = 80% Analysis Date = 12/04/15 Pct Recovery = 80% Analysis Date = 12/04/15 Pct Recovery = 80% Analysis Date = 11/29/15 Pct Recovery = 80% Analysis Date = 11/29/15 Pct Recovery = 80% Analysis Date = 11/24/15 Pct Recovery = 80% Analysis Date = 11/24/15 Pct Recovery = 80% Analysis Date = 11/20/15 Pct Recovery = 80% Analysis Date = 11/20/15 Pct Recovery = 80% Analysis Date = 11/15/15 Pct Recovery = 80% Analysis Date = 11/15/15 Pct Recovery = 80% Analysis Date = 11/10/15 Pct Recovery = 79% Analysis Date = 11/10/15 Pct Recovery = 79% Analysis Date = 11/06/15 Pct Recovery = 79% Analysis Date = 11/06/15 Pct Recovery = 79% Analysis Date = 11/01/15 Pct Recovery = 79% Analysis Date = 11/01/15 Pct Recovery = 79% Analysis Date = 10/27/15 Pct Recovery = 79% Analysis Date = 10/27/15 Pct Recovery = 79% Analysis Date = 10/22/15 Pct Recovery = 78% Analysis Date = 10/22/15 Pct Recovery = 78% Analysis Date = 10/18/15 Pct Recovery = 78% Analysis Date = 10/18/15 Pct Recovery = 78% Analysis Date = 10/13/15 Pct Recovery = 78% Analysis Date = 10/13/15 Pct Recovery = 78% Analysis Date = 10/08/15 Pct Recovery = 77% Analysis Date = 10/08/15 Pct Recovery = 77% Analysis Date = 10/04/15 Pct Recovery = 77% Analysis Date = 10/04/15 Pct Recovery = 77% Analysis Date = 09/29/15 Pct Recovery = 77% Analysis Date = 09/29/15 Pct Recovery = 77% Analysis Date = 09/24/15 Pct Recovery = 76% Analysis Date = 09/24/15 Pct Recovery = 76% Analysis Date = 09/19/15 Pct Recovery = 76% Analysis Date = 09/19/15 Pct Recovery = 76% Analysis Date = 09/15/15 Pct Recovery = 76% Analysis Date = 09/15/15 Pct Recovery = 76% Analysis Date = 09/10/15 Pct Recovery = 75% Analysis Date = 09/10/15 Pct Recovery = 75% Analysis Date = 09/05/15 Pct Recovery = 75% Analysis Date = 09/05/15 Pct Recovery = 75% Analysis Date = 09/01/15 Pct Recovery = 75% Analysis Date = 09/01/15 Pct Recovery = 75% Analysis Date = 08/27/15 Pct Recovery = 74% Analysis Date = 08/27/15 Pct Recovery = 74% Analysis Date = 08/22/15 Pct Recovery = 74% Analysis Date = 08/22/15 Pct Recovery = 74% Analysis Date = 08/17/15 Pct Recovery = 73% Analysis Date = 08/17/15 Pct Recovery = 73% Analysis Date = 08/13/15 Pct Recovery = 72% Analysis Date = 08/13/15 Pct Recovery = 72% Analysis Date = 08/08/15 Pct Recovery = 72% Analysis Date = 08/08/15 Pct Recovery = 72% Analysis Date = 08/03/15 Pct Recovery = 71% Analysis Date = 08/03/15 Pct Recovery = 71% Analysis Date = 07/29/15 Pct Recovery = 70% Analysis Date = 07/29/15 Pct Recovery = 70% Analysis Date = 07/25/15 Pct Recovery = 70% Analysis Date = 07/25/15 Pct Recovery = 70% Analysis Date = 07/20/15 Pct Recovery = 69% Analysis Date = 07/20/15 Pct Recovery = 69% Analysis Date = 07/15/15 Pct Recovery = 68% Analysis Date = 07/15/15 Pct Recovery = 68% Analysis Date = 07/11/15 Pct Recovery = 68% Analysis Date = 07/11/15 Pct Recovery = 68% Analysis Date = 07/06/15 Pct Recovery = 67% Analysis Date = 07/06/15 Pct Recovery = 67% Analysis Date = 07/01/15 Pct Recovery = 66% Analysis Date = 07/01/15 Pct Recovery = 66% Analysis Date = 06/26/15 Pct Recovery = 66% Analysis Date = 06/26/15 Pct Recovery = 66% Analysis Date = 06/22/15 Pct Recovery = 65% Analysis Date = 06/22/15 Pct Recovery = 65% Analysis Date = 06/17/15 Pct Recovery = 65% Analysis Date = 06/17/15 Pct Recovery = 65% Analysis Date = 06/12/15 Pct Recovery = 65% Analysis Date = 06/12/15 Pct Recovery = 65% Analysis Date = 06/08/15 Pct Recovery = 64% Analysis Date = 06/08/15 Pct Recovery = 64% Analysis Date = 06/03/15 Pct Recovery = 64% Analysis Date = 06/03/15 Pct Recovery = 64% Analysis Date = 05/29/15 Pct Recovery = 64% Analysis Date = 05/29/15 Pct Recovery = 64% Analysis Date = 05/24/15 Pct Recovery = 63% Analysis Date = 05/24/15 Pct Recovery = 63% Analysis Date = 05/20/15 Pct Recovery = 63% Analysis Date = 05/20/15 Pct Recovery = 63% Analysis Date = 05/15/15 Pct Recovery = 63% Analysis Date = 05/15/15 Pct Recovery = 63% Analysis Date = 05/10/15 Pct Recovery = 63% Analysis Date = 05/10/15 Pct Recovery = 63% Analysis Date = 05/06/15 Pct Recovery = 62% Analysis Date = 05/06/15 Pct Recovery = 62% Analysis Date = 05/01/15 Pct Recovery = 62% Analysis Date = 05/01/15 Pct Recovery = 62% Analysis Date = 04/26/15 Pct Recovery = 62% Analysis Date = 04/26/15 Pct Recovery = 62% Analysis Date = 04/21/15 Pct Recovery = 61% Analysis Date = 04/21/15 Pct Recovery = 61% Analysis Date = 04/17/15 Pct Recovery = 61% Analysis Date = 04/17/15 Pct Recovery = 61% Analysis Date = 04/12/15 Pct Recovery = 61% Analysis Date = 04/12/15 Pct Recovery = 61% Analysis Date = 04/07/15 Pct Recovery = 60% Analysis Date = 04/07/15 Pct Recovery = 60% Analysis Date = 04/02/15 Pct Recovery = 60% Analysis Date = 04/02/15 Pct Recovery = 60% Analysis Date = 03/29/15 Pct Recovery = 60% Analysis Date = 03/29/15 Pct Recovery = 60% Analysis Date = 03/24/15 Pct Recovery = 59% Analysis Date = 03/24/15 Pct Recovery = 59% Analysis Date = 03/19/15 Pct Recovery = 59% Analysis Date = 03/19/15 Pct Recovery = 59% Analysis Date = 03/15/15 Pct Recovery = 59% Analysis Date = 03/15/15 Pct Recovery = 59% Analysis Date = 03/10/15 Pct Recovery = 59% Analysis Date = 03/10/15 Pct Recovery = 59% Analysis Date = 03/05/15 Pct Recovery = 58% Analysis Date = 03/05/15 Pct Recovery = 58% Analysis Date = 02/28/15 Pct Recovery = 58% Analysis Date = 02/28/15 Pct Recovery = 58% Analysis Date = 02/24/15 Pct Recovery = 58% Analysis Date = 02/24/15 Pct Recovery = 58% Analysis Date = 02/19/15 Pct Recovery = 57% Analysis Date = 02/19/15 Pct Recovery = 57% Analysis Date = 02/14/15 Pct Recovery = 57% Analysis Date = 02/14/15 Pct Recovery = 57% Analysis Date = 02/10/15 Pct Recovery = 57% Analysis Date = 02/10/15 Pct Recovery = 57% Analysis Date = 02/05/15 Pct Recovery = 56% Analysis Date = 02/05/15 Pct Recovery = 56% Analysis Date = 01/31/15 Pct Recovery = 56% Analysis Date = 01/31/15 Pct Recovery = 56% Analysis Date = 01/26/15 Pct Recovery = 56% Analysis Date = 01/26/15 Pct Recovery = 56% Analysis Date = 01/22/15 Pct Recovery = 55% Analysis Date = 01/22/15 Pct Recovery = 55% Analysis Date = 01/17/15 Pct Recovery = 55% Analysis Date = 01/17/15 Pct Recovery = 55% Analysis Date = 01/12/15 Pct Recovery = 55% Analysis Date = 01/12/15 Pct Recovery = 55% Analysis Date = 01/08/15 Pct Recovery = 55% Analysis Date = 01/08/15 Pct Recovery = 55% Analysis Date = 01/03/15 Pct Recovery = 55% Analysis Date = 01/03/15 Pct Recovery = 55% Analysis Date = 12/29/14 Pct Recovery = 54% Analysis Date = 12/29/14 Pct Recovery = 54% Analysis Date = 12/24/14 Pct Recovery = 54% Analysis Date = 12/24/14 Pct Recovery = 54% Analysis Date = 12/20/14 Pct Recovery = 54% Analysis Date = 12/20/14 Pct Recovery = 54% Analysis Date = 12/15/14 Pct Recovery = 54% Analysis Date = 12/15/14 Pct Recovery = 54% Analysis Date = 12/10/14 Pct Recovery = 54% Analysis Date = 12/10/14 Pct Recovery = 54% Analysis Date = 12/05/14 Pct Recovery = 53% Analysis Date = 12/05/14 Pct Recovery = 53% Analysis Date = 12/01/14 Pct Recovery = 53% Analysis Date = 12/01/14 Pct Recovery = 53% Analysis Date = 11/26/14 Pct Recovery = 53% Analysis Date = 11/26/14 Pct Recovery = 53% Analysis Date = 11/21/14 Pct Recovery = 53% Analysis Date = 11/21/14 Pct Recovery = 53% Analysis Date = 11/17/14 Pct Recovery = 53% Analysis Date = 11/17/14 Pct Recovery = 53% Analysis Date = 11/12/14 Pct Recovery = 53% Analysis Date = 11/12/14 Pct Recovery = 53% Analysis Date = 11/07/14 Pct Recovery = 52% Analysis Date = 11/07/14 Pct Recovery = 52% Analysis Date = 11/02/14 Pct Recovery = 52% Analysis Date = 11/02/14 Pct Recovery = 52% Analysis Date = 10/29/14 Pct Recovery = 52% Analysis Date = 10/29/14 Pct Recovery = 52% Analysis Date = 10/24/14 Pct Recovery = 52% Analysis Date = 10/24/14 Pct Recovery = 52% Analysis Date = 10/19/14 Pct Recovery = 52% Analysis Date = 10/19/14 Pct Recovery = 52% Analysis Date = 10/15/14 Pct Recovery = 51% Analysis Date = 10/15/14 Pct Recovery = 51% Analysis Date = 10/10/14 Pct Recovery = 51% Analysis Date = 10/10/14 Pct Recovery = 51% Analysis Date = 10/05/14 Pct Recovery = 51% Analysis Date = 10/05/14 Pct Recovery = 51% Analysis Date = 09/30/14 Pct Recovery = 51% Analysis Date = 09/30/14 Pct Recovery = 51% Analysis Date = 09/26/14 Pct Recovery = 51% Analysis Date = 09/26/14 Pct Recovery = 51% Analysis Date = 09/21/14 Pct Recovery = 51% Analysis Date = 09/21/14 Pct Recovery = 51% Analysis Date = 09/16/14 Pct Recovery = 50% Analysis Date = 09/16/14 Pct Recovery = 50% Analysis Date = 09/12/14 Pct Recovery = 50% Analysis Date = 09/12/14 Pct Recovery = 50% Analysis Date = 09/07/14 Pct Recovery = 50% Analysis Date = 09/07/14 Pct Recovery = 50% Analysis Date = 09/02/14 Pct Recovery = 50% Analysis Date = 09/02/14 Pct Recovery = 50% Analysis Date = 08/28/14 Pct Recovery = 50% Analysis Date = 08/28/14 Pct Recovery = 50% Analysis Date = 08/24/14 Pct Recovery = 49% Analysis Date = 08/24/14 Pct Recovery = 49% Analysis Date = 08/19/14 Pct Recovery = 49% Analysis Date = 08/19/14 Pct Recovery = 49% Analysis Date = 08/14/14 Pct Recovery = 49% Analysis Date = 08/14/14 Pct Recovery = 49% Analysis Date = 08/09/14 Pct Recovery = 49% Analysis Date = 08/09/14 Pct Recovery = 49% Analysis Date = 08/05/14 Pct Recovery = 49% Analysis Date = 08/05/14 Pct Recovery = 49% Analysis Date = 07/31/14 Pct Recovery = 49% Analysis Date = 07/31/14 Pct Recovery = 49% Analysis Date = 07/26/14 Pct Recovery = 49% Analysis Date = 07/26/14 Pct Recovery = 49% Analysis Date = 07/22/14 Pct Recovery = 48% Analysis Date = 07/22/14 Pct Recovery = 48% Analysis Date = 07/17/14 Pct Recovery = 48% Analysis Date = 07/17/14 Pct Recovery = 48% Analysis Date = 07/12/14 Pct Recovery = 48% Analysis Date = 07/12/14 Pct Recovery = 48% Analysis Date = 07/07/14 Pct Recovery = 48% Analysis Date = 07/07/14 Pct Recovery = 48% Analysis Date = 07/03/14 Pct Recovery = 48% Analysis Date = 07/03/14 Pct Recovery = 48% Analysis Date = 06/28/14 Pct Recovery = 48% Analysis Date = 06/28/14 Pct Recovery = 48% Analysis Date = 06/23/14 Pct Recovery = 47% Analysis Date = 06/23/14 Pct Recovery = 47% Analysis Date = 06/19/14 Pct Recovery = 47% Analysis Date = 06/19/14 Pct Recovery = 47% Analysis Date = 06/14/14 Pct Recovery = 47% Analysis Date = 06/14/14 Pct Recovery = 47% Analysis Date = 06/09/14 Pct Recovery = 47% Analysis Date = 06/09/14 Pct Recovery = 47% Analysis Date = 06/04/14 Pct Recovery = 47% Analysis Date = 06/04/14 Pct Recovery = 47% Analysis Date = 05/31/14 Pct Recovery = 47% Analysis Date = 05/31/14 Pct Recovery = 47% Analysis Date = 05/26/14 Pct Recovery = 47% Analysis Date = 05/26/14 Pct Recovery = 47% Analysis Date = 05/21/14 Pct Recovery = 47% Analysis Date = 05/21/14 Pct Recovery = 47% Analysis Date = 05/17/14 Pct Recovery = 46% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
10-HYDROXY-AMITRIPTYLINE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 2 77% 30% 77% 31%
>= Reporting Level 51 69% 22% 67% 22%
Total 53 69% 22% 67% 22%

Sample Statistics
10-HYDROXY-AMITRIPTYLINE

Characteristic N % % Basis
Plotted 53 100% Spiked
Estimated Values 38 72% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 53 .  
False Negatives 0 0% 0 out of 53
Not Spiked 62 .  
False Positives 0 0% 0 out of 62

BQS OBSP Determination:
ABACAVIR
METHOD: 2440 , TESTIDCODE: 68022LCM56
Open Data Set

Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 74% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 72% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 33% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 36% Analysis Date = 01/17/16 SpikeMix = ERA 0406-15-09: 80 µl & ERA 0406-15-07A: 80 µl Pct Recovery = 64% Analysis Date = 11/24/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 68% Analysis Date = 10/01/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 69% Analysis Date = 11/05/15 SpikeMix = ERA 0406-15-08: 80 µl & Abs 052215: 80 µl Pct Recovery = 67% Analysis Date = 11/04/15 SpikeMix = Abs 052215: 80 µl & Abs 050115: 80 µl Pct Recovery = 66% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 63% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 64% Analysis Date = 09/24/16 SpikeMix = Crescent EN160610015: 80 µl & Abs 061416: 80 µl Pct Recovery = 72% Analysis Date = 09/24/16 SpikeMix = Abs 061416: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 69% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 30% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 30% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 35% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 35% Analysis Date = 04/29/15 SpikeMix = ERA 0319-14-05: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 75% Analysis Date = 03/11/15 SpikeMix = ERA 0318-14-02: 15 µl & Abs 041714: 15 µl Pct Recovery = 71% Analysis Date = 02/06/15 SpikeMix = Abs 041814: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 73% Analysis Date = 12/06/14 SpikeMix = ERA 0318-14-02: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 64% Analysis Date = 10/11/14 SpikeMix = ERA 0318-14-02: 60 µl & ERA 0319-14-04: 60 µl Pct Recovery = 55% Analysis Date = 08/21/14 SpikeMix = ERA 0318-14-02: 60 µl & Abs 041714: 60 µl Pct Recovery = 62% Analysis Date = 07/26/14 SpikeMix = ERA 0319-14-05: 60 µl & ERA 0318-14-02: 60 µl Pct Recovery = 68% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 55% Analysis Date = 12/07/14 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 61% Analysis Date = 10/25/14 SpikeMix = Abs 041614: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 58% Analysis Date = 06/22/14 SpikeMix = Abs 041814: 60 µl & Abs 041614: 60 µl Pct Recovery = 77% Analysis Date = 06/11/14 SpikeMix = Abs 041614: 60 µl & Abs 041714: 60 µl Pct Recovery = 54% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-08: 40 µl & ERA 0406-15-09: 40 µl Pct Recovery = 61% Analysis Date = 07/31/15 SpikeMix = ERA 0406-15-09: 40 µl & Abs 050115: 40 µl Pct Recovery = 72% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-08: 40 µl & Abs 052215: 40 µl Pct Recovery = 62% Analysis Date = 02/23/16 SpikeMix = Abs 052215: 40 µl & Abs 050115: 40 µl Pct Recovery = 68% Analysis Date = 09/10/15 SpikeMix = Abs 052215: 40 µl & ERA 0406-15-07A: 40 µl Pct Recovery = 62% Analysis Date = 07/31/15 SpikeMix = Abs 051315: 40 µl & Abs 052215: 40 µl Pct Recovery = 61% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 54% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 60% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 68% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 71% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 31% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 31% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 33% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 29% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 29% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 28% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 22% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 17% Analysis Date = 12/07/14 SpikeMix = ERA 0318-14-02: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 59% Analysis Date = 11/04/14 SpikeMix = Abs 041814: 8 µl & ERA 0318-14-02: 8 µl Pct Recovery = 61% Analysis Date = 04/30/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 58% Analysis Date = 02/10/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 70% Analysis Date = 10/24/14 SpikeMix = ERA 0319-14-05: 8 µl & Abs 041614: 8 µl Pct Recovery = 56% Analysis Date = 10/10/14 SpikeMix = Abs 041814: 30 µl & ERA 0318-14-02: 30 µl Pct Recovery = 52% Analysis Date = 08/30/14 SpikeMix = ERA 0318-14-02: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 67% Analysis Date = 07/20/14 SpikeMix = ERA 0318-14-02: 30 µl & Abs 041714: 30 µl Pct Recovery = 56% Analysis Date = 09/12/14 SpikeMix = Abs 041614: 30 µl & ERA 0319-14-04: 30 µl Pct Recovery = 36% Analysis Date = 07/13/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 53% Analysis Date = 06/28/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 49% Analysis Date = 05/30/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 57% Analysis Date = 05/17/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 58% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 64% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 68% Analysis Date = 11/24/15 SpikeMix = ERA 0406-15-09: 20 µl & Abs 050115: 20 µl Pct Recovery = 63% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-09: 20 µl Pct Recovery = 51% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 46% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 43% Analysis Date = 02/23/16 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 69% Analysis Date = 11/24/15 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 66% Analysis Date = 09/09/15 SpikeMix = ERA 0406-15-08: 20 µl & Abs 052215: 20 µl Pct Recovery = 60% Analysis Date = 08/27/15 SpikeMix = Abs 052215: 20 µl & Abs 050115: 20 µl Pct Recovery = 61% Analysis Date = 07/09/15 SpikeMix = Abs 050115: 20 µl & Abs 052215: 20 µl Pct Recovery = 58% Analysis Date = 06/26/15 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 57% Analysis Date = 04/09/16 SpikeMix = Abs 051315: 10 µl & ERA 0406-15-09: 10 µl Pct Recovery = 54% Analysis Date = 04/09/16 SpikeMix = Abs 051315: 10 µl & ERA 0406-15-09: 10 µl Pct Recovery = 58% Analysis Date = 01/18/17 Pct Recovery = 46% Analysis Date = 01/14/17 Pct Recovery = 46% Analysis Date = 01/14/17 Pct Recovery = 46% Analysis Date = 01/09/17 Pct Recovery = 46% Analysis Date = 01/09/17 Pct Recovery = 46% Analysis Date = 01/04/17 Pct Recovery = 46% Analysis Date = 01/04/17 Pct Recovery = 46% Analysis Date = 12/30/16 Pct Recovery = 46% Analysis Date = 12/30/16 Pct Recovery = 46% Analysis Date = 12/25/16 Pct Recovery = 46% Analysis Date = 12/25/16 Pct Recovery = 46% Analysis Date = 12/20/16 Pct Recovery = 46% Analysis Date = 12/20/16 Pct Recovery = 46% Analysis Date = 12/15/16 Pct Recovery = 46% Analysis Date = 12/15/16 Pct Recovery = 46% Analysis Date = 12/10/16 Pct Recovery = 46% Analysis Date = 12/10/16 Pct Recovery = 46% Analysis Date = 12/05/16 Pct Recovery = 46% Analysis Date = 12/05/16 Pct Recovery = 46% Analysis Date = 12/01/16 Pct Recovery = 46% Analysis Date = 12/01/16 Pct Recovery = 46% Analysis Date = 11/26/16 Pct Recovery = 46% Analysis Date = 11/26/16 Pct Recovery = 46% Analysis Date = 11/21/16 Pct Recovery = 46% Analysis Date = 11/21/16 Pct Recovery = 46% Analysis Date = 11/16/16 Pct Recovery = 46% Analysis Date = 11/16/16 Pct Recovery = 46% Analysis Date = 11/11/16 Pct Recovery = 46% Analysis Date = 11/11/16 Pct Recovery = 46% Analysis Date = 11/06/16 Pct Recovery = 46% Analysis Date = 11/06/16 Pct Recovery = 46% Analysis Date = 11/01/16 Pct Recovery = 47% Analysis Date = 11/01/16 Pct Recovery = 47% Analysis Date = 10/27/16 Pct Recovery = 47% Analysis Date = 10/27/16 Pct Recovery = 47% Analysis Date = 10/22/16 Pct Recovery = 47% Analysis Date = 10/22/16 Pct Recovery = 47% Analysis Date = 10/18/16 Pct Recovery = 47% Analysis Date = 10/18/16 Pct Recovery = 47% Analysis Date = 10/13/16 Pct Recovery = 47% Analysis Date = 10/13/16 Pct Recovery = 47% Analysis Date = 10/08/16 Pct Recovery = 47% Analysis Date = 10/08/16 Pct Recovery = 47% Analysis Date = 10/03/16 Pct Recovery = 47% Analysis Date = 10/03/16 Pct Recovery = 47% Analysis Date = 09/28/16 Pct Recovery = 47% Analysis Date = 09/28/16 Pct Recovery = 47% Analysis Date = 09/23/16 Pct Recovery = 47% Analysis Date = 09/23/16 Pct Recovery = 47% Analysis Date = 09/18/16 Pct Recovery = 48% Analysis Date = 09/18/16 Pct Recovery = 48% Analysis Date = 09/13/16 Pct Recovery = 48% Analysis Date = 09/13/16 Pct Recovery = 48% Analysis Date = 09/08/16 Pct Recovery = 48% Analysis Date = 09/08/16 Pct Recovery = 48% Analysis Date = 09/04/16 Pct Recovery = 48% Analysis Date = 09/04/16 Pct Recovery = 48% Analysis Date = 08/30/16 Pct Recovery = 48% Analysis Date = 08/30/16 Pct Recovery = 48% Analysis Date = 08/25/16 Pct Recovery = 48% Analysis Date = 08/25/16 Pct Recovery = 48% Analysis Date = 08/20/16 Pct Recovery = 49% Analysis Date = 08/20/16 Pct Recovery = 49% Analysis Date = 08/15/16 Pct Recovery = 49% Analysis Date = 08/15/16 Pct Recovery = 49% Analysis Date = 08/10/16 Pct Recovery = 49% Analysis Date = 08/10/16 Pct Recovery = 49% Analysis Date = 08/05/16 Pct Recovery = 49% Analysis Date = 08/05/16 Pct Recovery = 49% Analysis Date = 07/31/16 Pct Recovery = 49% Analysis Date = 07/31/16 Pct Recovery = 49% Analysis Date = 07/26/16 Pct Recovery = 49% Analysis Date = 07/26/16 Pct Recovery = 49% Analysis Date = 07/22/16 Pct Recovery = 50% Analysis Date = 07/22/16 Pct Recovery = 50% Analysis Date = 07/17/16 Pct Recovery = 50% Analysis Date = 07/17/16 Pct Recovery = 50% Analysis Date = 07/12/16 Pct Recovery = 50% Analysis Date = 07/12/16 Pct Recovery = 50% Analysis Date = 07/07/16 Pct Recovery = 50% Analysis Date = 07/07/16 Pct Recovery = 50% Analysis Date = 07/02/16 Pct Recovery = 50% Analysis Date = 07/02/16 Pct Recovery = 50% Analysis Date = 06/27/16 Pct Recovery = 51% Analysis Date = 06/27/16 Pct Recovery = 51% Analysis Date = 06/22/16 Pct Recovery = 51% Analysis Date = 06/22/16 Pct Recovery = 51% Analysis Date = 06/17/16 Pct Recovery = 51% Analysis Date = 06/17/16 Pct Recovery = 51% Analysis Date = 06/12/16 Pct Recovery = 51% Analysis Date = 06/12/16 Pct Recovery = 51% Analysis Date = 06/08/16 Pct Recovery = 51% Analysis Date = 06/08/16 Pct Recovery = 51% Analysis Date = 06/03/16 Pct Recovery = 52% Analysis Date = 06/03/16 Pct Recovery = 52% Analysis Date = 05/29/16 Pct Recovery = 52% Analysis Date = 05/29/16 Pct Recovery = 52% Analysis Date = 05/24/16 Pct Recovery = 52% Analysis Date = 05/24/16 Pct Recovery = 52% Analysis Date = 05/19/16 Pct Recovery = 52% Analysis Date = 05/19/16 Pct Recovery = 52% Analysis Date = 05/14/16 Pct Recovery = 52% Analysis Date = 05/14/16 Pct Recovery = 52% Analysis Date = 05/09/16 Pct Recovery = 53% Analysis Date = 05/09/16 Pct Recovery = 53% Analysis Date = 05/04/16 Pct Recovery = 53% Analysis Date = 05/04/16 Pct Recovery = 53% Analysis Date = 04/29/16 Pct Recovery = 53% Analysis Date = 04/29/16 Pct Recovery = 53% Analysis Date = 04/25/16 Pct Recovery = 53% Analysis Date = 04/25/16 Pct Recovery = 53% Analysis Date = 04/20/16 Pct Recovery = 53% Analysis Date = 04/20/16 Pct Recovery = 53% Analysis Date = 04/15/16 Pct Recovery = 54% Analysis Date = 04/15/16 Pct Recovery = 54% Analysis Date = 04/10/16 Pct Recovery = 54% Analysis Date = 04/10/16 Pct Recovery = 54% Analysis Date = 04/05/16 Pct Recovery = 54% Analysis Date = 04/05/16 Pct Recovery = 54% Analysis Date = 03/31/16 Pct Recovery = 54% Analysis Date = 03/31/16 Pct Recovery = 54% Analysis Date = 03/26/16 Pct Recovery = 55% Analysis Date = 03/26/16 Pct Recovery = 55% Analysis Date = 03/21/16 Pct Recovery = 55% Analysis Date = 03/21/16 Pct Recovery = 55% Analysis Date = 03/16/16 Pct Recovery = 55% Analysis Date = 03/16/16 Pct Recovery = 55% Analysis Date = 03/12/16 Pct Recovery = 55% Analysis Date = 03/12/16 Pct Recovery = 55% Analysis Date = 03/07/16 Pct Recovery = 56% Analysis Date = 03/07/16 Pct Recovery = 56% Analysis Date = 03/02/16 Pct Recovery = 56% Analysis Date = 03/02/16 Pct Recovery = 56% Analysis Date = 02/26/16 Pct Recovery = 56% Analysis Date = 02/26/16 Pct Recovery = 56% Analysis Date = 02/21/16 Pct Recovery = 56% Analysis Date = 02/21/16 Pct Recovery = 56% Analysis Date = 02/16/16 Pct Recovery = 57% Analysis Date = 02/16/16 Pct Recovery = 57% Analysis Date = 02/11/16 Pct Recovery = 57% Analysis Date = 02/11/16 Pct Recovery = 57% Analysis Date = 02/06/16 Pct Recovery = 57% Analysis Date = 02/06/16 Pct Recovery = 57% Analysis Date = 02/01/16 Pct Recovery = 57% Analysis Date = 02/01/16 Pct Recovery = 57% Analysis Date = 01/28/16 Pct Recovery = 58% Analysis Date = 01/28/16 Pct Recovery = 58% Analysis Date = 01/23/16 Pct Recovery = 58% Analysis Date = 01/23/16 Pct Recovery = 58% Analysis Date = 01/18/16 Pct Recovery = 58% Analysis Date = 01/18/16 Pct Recovery = 58% Analysis Date = 01/13/16 Pct Recovery = 58% Analysis Date = 01/13/16 Pct Recovery = 58% Analysis Date = 01/08/16 Pct Recovery = 59% Analysis Date = 01/08/16 Pct Recovery = 59% Analysis Date = 01/03/16 Pct Recovery = 59% Analysis Date = 01/03/16 Pct Recovery = 59% Analysis Date = 12/29/15 Pct Recovery = 59% Analysis Date = 12/29/15 Pct Recovery = 59% Analysis Date = 12/24/15 Pct Recovery = 59% Analysis Date = 12/24/15 Pct Recovery = 59% Analysis Date = 12/19/15 Pct Recovery = 60% Analysis Date = 12/19/15 Pct Recovery = 60% Analysis Date = 12/15/15 Pct Recovery = 60% Analysis Date = 12/15/15 Pct Recovery = 60% Analysis Date = 12/10/15 Pct Recovery = 60% Analysis Date = 12/10/15 Pct Recovery = 60% Analysis Date = 12/05/15 Pct Recovery = 60% Analysis Date = 12/05/15 Pct Recovery = 60% Analysis Date = 11/30/15 Pct Recovery = 61% Analysis Date = 11/30/15 Pct Recovery = 61% Analysis Date = 11/25/15 Pct Recovery = 61% Analysis Date = 11/25/15 Pct Recovery = 61% Analysis Date = 11/20/15 Pct Recovery = 61% Analysis Date = 11/20/15 Pct Recovery = 61% Analysis Date = 11/15/15 Pct Recovery = 62% Analysis Date = 11/15/15 Pct Recovery = 62% Analysis Date = 11/10/15 Pct Recovery = 62% Analysis Date = 11/10/15 Pct Recovery = 62% Analysis Date = 11/05/15 Pct Recovery = 62% Analysis Date = 11/05/15 Pct Recovery = 62% Analysis Date = 11/01/15 Pct Recovery = 62% Analysis Date = 11/01/15 Pct Recovery = 62% Analysis Date = 10/27/15 Pct Recovery = 62% Analysis Date = 10/27/15 Pct Recovery = 62% Analysis Date = 10/22/15 Pct Recovery = 62% Analysis Date = 10/22/15 Pct Recovery = 62% Analysis Date = 10/17/15 Pct Recovery = 63% Analysis Date = 10/17/15 Pct Recovery = 63% Analysis Date = 10/12/15 Pct Recovery = 63% Analysis Date = 10/12/15 Pct Recovery = 63% Analysis Date = 10/07/15 Pct Recovery = 63% Analysis Date = 10/07/15 Pct Recovery = 63% Analysis Date = 10/02/15 Pct Recovery = 63% Analysis Date = 10/02/15 Pct Recovery = 63% Analysis Date = 09/27/15 Pct Recovery = 63% Analysis Date = 09/27/15 Pct Recovery = 63% Analysis Date = 09/22/15 Pct Recovery = 63% Analysis Date = 09/22/15 Pct Recovery = 63% Analysis Date = 09/17/15 Pct Recovery = 63% Analysis Date = 09/17/15 Pct Recovery = 63% Analysis Date = 09/13/15 Pct Recovery = 63% Analysis Date = 09/13/15 Pct Recovery = 63% Analysis Date = 09/08/15 Pct Recovery = 63% Analysis Date = 09/08/15 Pct Recovery = 63% Analysis Date = 09/03/15 Pct Recovery = 63% Analysis Date = 09/03/15 Pct Recovery = 63% Analysis Date = 08/29/15 Pct Recovery = 63% Analysis Date = 08/29/15 Pct Recovery = 63% Analysis Date = 08/24/15 Pct Recovery = 63% Analysis Date = 08/24/15 Pct Recovery = 63% Analysis Date = 08/19/15 Pct Recovery = 63% Analysis Date = 08/19/15 Pct Recovery = 63% Analysis Date = 08/14/15 Pct Recovery = 63% Analysis Date = 08/14/15 Pct Recovery = 63% Analysis Date = 08/09/15 Pct Recovery = 63% Analysis Date = 08/09/15 Pct Recovery = 63% Analysis Date = 08/04/15 Pct Recovery = 63% Analysis Date = 08/04/15 Pct Recovery = 63% Analysis Date = 07/31/15 Pct Recovery = 63% Analysis Date = 07/31/15 Pct Recovery = 63% Analysis Date = 07/26/15 Pct Recovery = 63% Analysis Date = 07/26/15 Pct Recovery = 63% Analysis Date = 07/21/15 Pct Recovery = 63% Analysis Date = 07/21/15 Pct Recovery = 63% Analysis Date = 07/16/15 Pct Recovery = 63% Analysis Date = 07/16/15 Pct Recovery = 63% Analysis Date = 07/11/15 Pct Recovery = 63% Analysis Date = 07/11/15 Pct Recovery = 63% Analysis Date = 07/06/15 Pct Recovery = 63% Analysis Date = 07/06/15 Pct Recovery = 63% Analysis Date = 07/01/15 Pct Recovery = 63% Analysis Date = 07/01/15 Pct Recovery = 63% Analysis Date = 06/26/15 Pct Recovery = 63% Analysis Date = 06/26/15 Pct Recovery = 63% Analysis Date = 06/21/15 Pct Recovery = 63% Analysis Date = 06/21/15 Pct Recovery = 63% Analysis Date = 06/17/15 Pct Recovery = 63% Analysis Date = 06/17/15 Pct Recovery = 63% Analysis Date = 06/12/15 Pct Recovery = 63% Analysis Date = 06/12/15 Pct Recovery = 63% Analysis Date = 06/07/15 Pct Recovery = 63% Analysis Date = 06/07/15 Pct Recovery = 63% Analysis Date = 06/02/15 Pct Recovery = 63% Analysis Date = 06/02/15 Pct Recovery = 63% Analysis Date = 05/28/15 Pct Recovery = 63% Analysis Date = 05/28/15 Pct Recovery = 63% Analysis Date = 05/23/15 Pct Recovery = 63% Analysis Date = 05/23/15 Pct Recovery = 63% Analysis Date = 05/18/15 Pct Recovery = 63% Analysis Date = 05/18/15 Pct Recovery = 63% Analysis Date = 05/13/15 Pct Recovery = 62% Analysis Date = 05/13/15 Pct Recovery = 62% Analysis Date = 05/08/15 Pct Recovery = 62% Analysis Date = 05/08/15 Pct Recovery = 62% Analysis Date = 05/04/15 Pct Recovery = 62% Analysis Date = 05/04/15 Pct Recovery = 62% Analysis Date = 04/29/15 Pct Recovery = 62% Analysis Date = 04/29/15 Pct Recovery = 62% Analysis Date = 04/24/15 Pct Recovery = 62% Analysis Date = 04/24/15 Pct Recovery = 62% Analysis Date = 04/19/15 Pct Recovery = 62% Analysis Date = 04/19/15 Pct Recovery = 62% Analysis Date = 04/14/15 Pct Recovery = 62% Analysis Date = 04/14/15 Pct Recovery = 62% Analysis Date = 04/09/15 Pct Recovery = 62% Analysis Date = 04/09/15 Pct Recovery = 62% Analysis Date = 04/04/15 Pct Recovery = 62% Analysis Date = 04/04/15 Pct Recovery = 62% Analysis Date = 03/30/15 Pct Recovery = 62% Analysis Date = 03/30/15 Pct Recovery = 62% Analysis Date = 03/25/15 Pct Recovery = 62% Analysis Date = 03/25/15 Pct Recovery = 62% Analysis Date = 03/21/15 Pct Recovery = 62% Analysis Date = 03/21/15 Pct Recovery = 62% Analysis Date = 03/16/15 Pct Recovery = 62% Analysis Date = 03/16/15 Pct Recovery = 62% Analysis Date = 03/11/15 Pct Recovery = 62% Analysis Date = 03/11/15 Pct Recovery = 62% Analysis Date = 03/06/15 Pct Recovery = 62% Analysis Date = 03/06/15 Pct Recovery = 62% Analysis Date = 03/01/15 Pct Recovery = 61% Analysis Date = 03/01/15 Pct Recovery = 61% Analysis Date = 02/24/15 Pct Recovery = 61% Analysis Date = 02/24/15 Pct Recovery = 61% Analysis Date = 02/19/15 Pct Recovery = 61% Analysis Date = 02/19/15 Pct Recovery = 61% Analysis Date = 02/14/15 Pct Recovery = 61% Analysis Date = 02/14/15 Pct Recovery = 61% Analysis Date = 02/09/15 Pct Recovery = 61% Analysis Date = 02/09/15 Pct Recovery = 61% Analysis Date = 02/05/15 Pct Recovery = 61% Analysis Date = 02/05/15 Pct Recovery = 61% Analysis Date = 01/31/15 Pct Recovery = 61% Analysis Date = 01/31/15 Pct Recovery = 61% Analysis Date = 01/26/15 Pct Recovery = 61% Analysis Date = 01/26/15 Pct Recovery = 61% Analysis Date = 01/21/15 Pct Recovery = 61% Analysis Date = 01/21/15 Pct Recovery = 61% Analysis Date = 01/16/15 Pct Recovery = 61% Analysis Date = 01/16/15 Pct Recovery = 61% Analysis Date = 01/11/15 Pct Recovery = 61% Analysis Date = 01/11/15 Pct Recovery = 61% Analysis Date = 01/06/15 Pct Recovery = 61% Analysis Date = 01/06/15 Pct Recovery = 61% Analysis Date = 01/01/15 Pct Recovery = 61% Analysis Date = 01/01/15 Pct Recovery = 61% Analysis Date = 12/27/14 Pct Recovery = 61% Analysis Date = 12/27/14 Pct Recovery = 61% Analysis Date = 12/23/14 Pct Recovery = 61% Analysis Date = 12/23/14 Pct Recovery = 61% Analysis Date = 12/18/14 Pct Recovery = 60% Analysis Date = 12/18/14 Pct Recovery = 60% Analysis Date = 12/13/14 Pct Recovery = 60% Analysis Date = 12/13/14 Pct Recovery = 60% Analysis Date = 12/08/14 Pct Recovery = 60% Analysis Date = 12/08/14 Pct Recovery = 60% Analysis Date = 12/03/14 Pct Recovery = 60% Analysis Date = 12/03/14 Pct Recovery = 60% Analysis Date = 11/28/14 Pct Recovery = 60% Analysis Date = 11/28/14 Pct Recovery = 60% Analysis Date = 11/23/14 Pct Recovery = 60% Analysis Date = 11/23/14 Pct Recovery = 60% Analysis Date = 11/18/14 Pct Recovery = 60% Analysis Date = 11/18/14 Pct Recovery = 60% Analysis Date = 11/13/14 Pct Recovery = 60% Analysis Date = 11/13/14 Pct Recovery = 60% Analysis Date = 11/09/14 Pct Recovery = 60% Analysis Date = 11/09/14 Pct Recovery = 60% Analysis Date = 11/04/14 Pct Recovery = 60% Analysis Date = 11/04/14 Pct Recovery = 60% Analysis Date = 10/30/14 Pct Recovery = 60% Analysis Date = 10/30/14 Pct Recovery = 60% Analysis Date = 10/25/14 Pct Recovery = 60% Analysis Date = 10/25/14 Pct Recovery = 60% Analysis Date = 10/20/14 Pct Recovery = 60% Analysis Date = 10/20/14 Pct Recovery = 60% Analysis Date = 10/15/14 Pct Recovery = 60% Analysis Date = 10/15/14 Pct Recovery = 60% Analysis Date = 10/10/14 Pct Recovery = 59% Analysis Date = 10/10/14 Pct Recovery = 59% Analysis Date = 10/05/14 Pct Recovery = 59% Analysis Date = 10/05/14 Pct Recovery = 59% Analysis Date = 09/30/14 Pct Recovery = 59% Analysis Date = 09/30/14 Pct Recovery = 59% Analysis Date = 09/26/14 Pct Recovery = 59% Analysis Date = 09/26/14 Pct Recovery = 59% Analysis Date = 09/21/14 Pct Recovery = 59% Analysis Date = 09/21/14 Pct Recovery = 59% Analysis Date = 09/16/14 Pct Recovery = 59% Analysis Date = 09/16/14 Pct Recovery = 59% Analysis Date = 09/11/14 Pct Recovery = 59% Analysis Date = 09/11/14 Pct Recovery = 59% Analysis Date = 09/06/14 Pct Recovery = 59% Analysis Date = 09/06/14 Pct Recovery = 59% Analysis Date = 09/01/14 Pct Recovery = 59% Analysis Date = 09/01/14 Pct Recovery = 59% Analysis Date = 08/27/14 Pct Recovery = 59% Analysis Date = 08/27/14 Pct Recovery = 59% Analysis Date = 08/22/14 Pct Recovery = 59% Analysis Date = 08/22/14 Pct Recovery = 59% Analysis Date = 08/17/14 Pct Recovery = 59% Analysis Date = 08/17/14 Pct Recovery = 59% Analysis Date = 08/13/14 Pct Recovery = 59% Analysis Date = 08/13/14 Pct Recovery = 59% Analysis Date = 08/08/14 Pct Recovery = 58% Analysis Date = 08/08/14 Pct Recovery = 58% Analysis Date = 08/03/14 Pct Recovery = 58% Analysis Date = 08/03/14 Pct Recovery = 58% Analysis Date = 07/29/14 Pct Recovery = 58% Analysis Date = 07/29/14 Pct Recovery = 58% Analysis Date = 07/24/14 Pct Recovery = 58% Analysis Date = 07/24/14 Pct Recovery = 58% Analysis Date = 07/19/14 Pct Recovery = 58% Analysis Date = 07/19/14 Pct Recovery = 58% Analysis Date = 07/14/14 Pct Recovery = 58% Analysis Date = 07/14/14 Pct Recovery = 58% Analysis Date = 07/09/14 Pct Recovery = 58% Analysis Date = 07/09/14 Pct Recovery = 58% Analysis Date = 07/04/14 Pct Recovery = 58% Analysis Date = 07/04/14 Pct Recovery = 58% Analysis Date = 06/30/14 Pct Recovery = 58% Analysis Date = 06/30/14 Pct Recovery = 58% Analysis Date = 06/25/14 Pct Recovery = 58% Analysis Date = 06/25/14 Pct Recovery = 58% Analysis Date = 06/20/14 Pct Recovery = 58% Analysis Date = 06/20/14 Pct Recovery = 58% Analysis Date = 06/15/14 Pct Recovery = 58% Analysis Date = 06/15/14 Pct Recovery = 58% Analysis Date = 06/10/14 Pct Recovery = 58% Analysis Date = 06/10/14 Pct Recovery = 58% Analysis Date = 06/05/14 Pct Recovery = 57% Analysis Date = 06/05/14 Pct Recovery = 57% Analysis Date = 05/31/14 Pct Recovery = 57% Analysis Date = 05/31/14 Pct Recovery = 57% Analysis Date = 05/26/14 Pct Recovery = 57% Analysis Date = 05/26/14 Pct Recovery = 57% Analysis Date = 05/21/14 Pct Recovery = 57% Analysis Date = 05/21/14 Pct Recovery = 57% Analysis Date = 05/17/14 Pct Recovery = 57% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
ABACAVIR

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 2 56% 3% 56% 3%
>= Reporting Level 72 56% 15% 60% 13%
Total 74 56% 15% 60% 12%

Sample Statistics
ABACAVIR

Characteristic N % % Basis
Plotted 74 99% Spiked
Estimated Values 4 5% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 75 .  
False Negatives 1 1% 1 out of 75
Not Spiked 40 .  
False Positives 0 0% 0 out of 40

BQS OBSP Determination:
ACETAMINOPHEN
METHOD: 2440 , TESTIDCODE: 67436LCM56
Open Data Set

Analysis Date = 04/10/15 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 729% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 76% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 85% Analysis Date = 01/17/16 SpikeMix = ERA 0406-15-09: 80 µl & ERA 0406-15-07A: 80 µl Pct Recovery = 89% Analysis Date = 11/24/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 85% Analysis Date = 11/05/15 SpikeMix = ERA 0406-15-08: 80 µl & Abs 052215: 80 µl Pct Recovery = 84% Analysis Date = 11/04/15 SpikeMix = Abs 052215: 80 µl & Abs 050115: 80 µl Pct Recovery = 89% Analysis Date = 09/24/16 SpikeMix = Crescent EN160610015: 80 µl & Abs 061416: 80 µl Pct Recovery = 80% Analysis Date = 09/24/16 SpikeMix = Abs 061416: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 80% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 99% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 88% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 99% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 90% Analysis Date = 11/18/16 SpikeMix = ERA 04281604: 80 µl & ERA 04281603: 80 µl Pct Recovery = 80% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & ERA 04281604: 80 µl Pct Recovery = 86% Analysis Date = 05/07/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 92% Analysis Date = 04/29/15 SpikeMix = ERA 0319-14-05: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 110% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 77% Analysis Date = 01/16/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 89% Analysis Date = 12/07/14 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 75% Analysis Date = 12/06/14 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 69% Analysis Date = 08/28/14 SpikeMix = ERA 0319-14-04: 60 µl & ERA 0319-14-05: 60 µl Pct Recovery = 58% Analysis Date = 07/26/14 SpikeMix = ERA 0319-14-05: 60 µl & ERA 0318-14-02: 60 µl Pct Recovery = 81% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-04: 15 µl & Abs 041814: 15 µl Pct Recovery = 77% Analysis Date = 02/06/15 SpikeMix = Abs 041814: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 79% Analysis Date = 07/12/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 65% Analysis Date = 05/21/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 71% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-08: 40 µl & ERA 0406-15-09: 40 µl Pct Recovery = 74% Analysis Date = 07/31/15 SpikeMix = ERA 0406-15-09: 40 µl & Abs 050115: 40 µl Pct Recovery = 133% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-08: 40 µl & Abs 052215: 40 µl Pct Recovery = 63% Analysis Date = 02/23/16 SpikeMix = Abs 052215: 40 µl & Abs 050115: 40 µl Pct Recovery = 110% Analysis Date = 09/10/15 SpikeMix = Abs 052215: 40 µl & ERA 0406-15-07A: 40 µl Pct Recovery = 92% Analysis Date = 07/31/15 SpikeMix = Abs 051315: 40 µl & Abs 052215: 40 µl Pct Recovery = 106% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 124% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 121% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 83% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 101% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 80% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 101% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 79% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 73% Analysis Date = 11/04/14 SpikeMix = Abs 041714: 8 µl & ERA 0319-14-05: 8 µl Pct Recovery = 100% Analysis Date = 10/24/14 SpikeMix = ERA 0319-14-05: 8 µl & Abs 041614: 8 µl Pct Recovery = 77% Analysis Date = 11/04/14 SpikeMix = Abs 041814: 8 µl & ERA 0318-14-02: 8 µl Pct Recovery = 84% Analysis Date = 10/11/14 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 50% Analysis Date = 04/23/14 SpikeMix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.2: 20 µl Pct Recovery = 55% Analysis Date = 08/30/14 SpikeMix = ERA 0318-14-02: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 97% Analysis Date = 08/16/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 49% Analysis Date = 07/13/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 58% Analysis Date = 10/10/14 SpikeMix = Abs 041714: 30 µl & Abs 041814: 30 µl Pct Recovery = 53% Analysis Date = 10/10/14 SpikeMix = Abs 041814: 30 µl & ERA 0318-14-02: 30 µl Pct Recovery = 52% Analysis Date = 07/13/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 61% Analysis Date = 05/30/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 85% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 100% Analysis Date = 11/24/15 SpikeMix = ERA 0406-15-09: 20 µl & Abs 050115: 20 µl Pct Recovery = 80% Analysis Date = 02/23/16 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 92% Analysis Date = 11/24/15 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 88% Analysis Date = 09/09/15 SpikeMix = ERA 0406-15-08: 20 µl & Abs 052215: 20 µl Pct Recovery = 88% Analysis Date = 08/27/15 SpikeMix = Abs 052215: 20 µl & Abs 050115: 20 µl Pct Recovery = 79% Analysis Date = 06/26/15 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 80% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 85% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 90% Analysis Date = 04/09/16 SpikeMix = Abs 051315: 10 µl & ERA 0406-15-09: 10 µl Pct Recovery = 50% Analysis Date = 11/18/16 Pct Recovery = 89% Analysis Date = 11/13/16 Pct Recovery = 89% Analysis Date = 11/13/16 Pct Recovery = 89% Analysis Date = 11/08/16 Pct Recovery = 89% Analysis Date = 11/08/16 Pct Recovery = 89% Analysis Date = 11/03/16 Pct Recovery = 89% Analysis Date = 11/03/16 Pct Recovery = 89% Analysis Date = 10/30/16 Pct Recovery = 89% Analysis Date = 10/30/16 Pct Recovery = 89% Analysis Date = 10/25/16 Pct Recovery = 89% Analysis Date = 10/25/16 Pct Recovery = 89% Analysis Date = 10/20/16 Pct Recovery = 89% Analysis Date = 10/20/16 Pct Recovery = 89% Analysis Date = 10/16/16 Pct Recovery = 89% Analysis Date = 10/16/16 Pct Recovery = 89% Analysis Date = 10/11/16 Pct Recovery = 89% Analysis Date = 10/11/16 Pct Recovery = 89% Analysis Date = 10/06/16 Pct Recovery = 89% Analysis Date = 10/06/16 Pct Recovery = 89% Analysis Date = 10/02/16 Pct Recovery = 89% Analysis Date = 10/02/16 Pct Recovery = 89% Analysis Date = 09/27/16 Pct Recovery = 89% Analysis Date = 09/27/16 Pct Recovery = 89% Analysis Date = 09/22/16 Pct Recovery = 89% Analysis Date = 09/22/16 Pct Recovery = 89% Analysis Date = 09/17/16 Pct Recovery = 89% Analysis Date = 09/17/16 Pct Recovery = 89% Analysis Date = 09/13/16 Pct Recovery = 89% Analysis Date = 09/13/16 Pct Recovery = 89% Analysis Date = 09/08/16 Pct Recovery = 89% Analysis Date = 09/08/16 Pct Recovery = 89% Analysis Date = 09/03/16 Pct Recovery = 89% Analysis Date = 09/03/16 Pct Recovery = 89% Analysis Date = 08/30/16 Pct Recovery = 89% Analysis Date = 08/30/16 Pct Recovery = 89% Analysis Date = 08/25/16 Pct Recovery = 89% Analysis Date = 08/25/16 Pct Recovery = 89% Analysis Date = 08/20/16 Pct Recovery = 89% Analysis Date = 08/20/16 Pct Recovery = 89% Analysis Date = 08/16/16 Pct Recovery = 89% Analysis Date = 08/16/16 Pct Recovery = 89% Analysis Date = 08/11/16 Pct Recovery = 89% Analysis Date = 08/11/16 Pct Recovery = 89% Analysis Date = 08/06/16 Pct Recovery = 89% Analysis Date = 08/06/16 Pct Recovery = 89% Analysis Date = 08/01/16 Pct Recovery = 89% Analysis Date = 08/01/16 Pct Recovery = 89% Analysis Date = 07/28/16 Pct Recovery = 89% Analysis Date = 07/28/16 Pct Recovery = 89% Analysis Date = 07/23/16 Pct Recovery = 88% Analysis Date = 07/23/16 Pct Recovery = 88% Analysis Date = 07/18/16 Pct Recovery = 88% Analysis Date = 07/18/16 Pct Recovery = 88% Analysis Date = 07/14/16 Pct Recovery = 88% Analysis Date = 07/14/16 Pct Recovery = 88% Analysis Date = 07/09/16 Pct Recovery = 88% Analysis Date = 07/09/16 Pct Recovery = 88% Analysis Date = 07/04/16 Pct Recovery = 88% Analysis Date = 07/04/16 Pct Recovery = 88% Analysis Date = 06/30/16 Pct Recovery = 88% Analysis Date = 06/30/16 Pct Recovery = 88% Analysis Date = 06/25/16 Pct Recovery = 88% Analysis Date = 06/25/16 Pct Recovery = 88% Analysis Date = 06/20/16 Pct Recovery = 88% Analysis Date = 06/20/16 Pct Recovery = 88% Analysis Date = 06/15/16 Pct Recovery = 88% Analysis Date = 06/15/16 Pct Recovery = 88% Analysis Date = 06/11/16 Pct Recovery = 88% Analysis Date = 06/11/16 Pct Recovery = 88% Analysis Date = 06/06/16 Pct Recovery = 88% Analysis Date = 06/06/16 Pct Recovery = 88% Analysis Date = 06/01/16 Pct Recovery = 88% Analysis Date = 06/01/16 Pct Recovery = 88% Analysis Date = 05/28/16 Pct Recovery = 88% Analysis Date = 05/28/16 Pct Recovery = 88% Analysis Date = 05/23/16 Pct Recovery = 88% Analysis Date = 05/23/16 Pct Recovery = 88% Analysis Date = 05/18/16 Pct Recovery = 88% Analysis Date = 05/18/16 Pct Recovery = 88% Analysis Date = 05/14/16 Pct Recovery = 88% Analysis Date = 05/14/16 Pct Recovery = 88% Analysis Date = 05/09/16 Pct Recovery = 88% Analysis Date = 05/09/16 Pct Recovery = 88% Analysis Date = 05/04/16 Pct Recovery = 88% Analysis Date = 05/04/16 Pct Recovery = 88% Analysis Date = 04/29/16 Pct Recovery = 88% Analysis Date = 04/29/16 Pct Recovery = 88% Analysis Date = 04/25/16 Pct Recovery = 88% Analysis Date = 04/25/16 Pct Recovery = 88% Analysis Date = 04/20/16 Pct Recovery = 88% Analysis Date = 04/20/16 Pct Recovery = 88% Analysis Date = 04/15/16 Pct Recovery = 88% Analysis Date = 04/15/16 Pct Recovery = 88% Analysis Date = 04/11/16 Pct Recovery = 88% Analysis Date = 04/11/16 Pct Recovery = 88% Analysis Date = 04/06/16 Pct Recovery = 88% Analysis Date = 04/06/16 Pct Recovery = 88% Analysis Date = 04/01/16 Pct Recovery = 88% Analysis Date = 04/01/16 Pct Recovery = 88% Analysis Date = 03/28/16 Pct Recovery = 87% Analysis Date = 03/28/16 Pct Recovery = 87% Analysis Date = 03/23/16 Pct Recovery = 87% Analysis Date = 03/23/16 Pct Recovery = 87% Analysis Date = 03/18/16 Pct Recovery = 87% Analysis Date = 03/18/16 Pct Recovery = 87% Analysis Date = 03/13/16 Pct Recovery = 87% Analysis Date = 03/13/16 Pct Recovery = 87% Analysis Date = 03/09/16 Pct Recovery = 87% Analysis Date = 03/09/16 Pct Recovery = 87% Analysis Date = 03/04/16 Pct Recovery = 87% Analysis Date = 03/04/16 Pct Recovery = 87% Analysis Date = 02/28/16 Pct Recovery = 87% Analysis Date = 02/28/16 Pct Recovery = 87% Analysis Date = 02/24/16 Pct Recovery = 87% Analysis Date = 02/24/16 Pct Recovery = 87% Analysis Date = 02/19/16 Pct Recovery = 87% Analysis Date = 02/19/16 Pct Recovery = 87% Analysis Date = 02/14/16 Pct Recovery = 88% Analysis Date = 02/14/16 Pct Recovery = 88% Analysis Date = 02/10/16 Pct Recovery = 88% Analysis Date = 02/10/16 Pct Recovery = 88% Analysis Date = 02/05/16 Pct Recovery = 88% Analysis Date = 02/05/16 Pct Recovery = 88% Analysis Date = 01/31/16 Pct Recovery = 89% Analysis Date = 01/31/16 Pct Recovery = 89% Analysis Date = 01/26/16 Pct Recovery = 89% Analysis Date = 01/26/16 Pct Recovery = 89% Analysis Date = 01/22/16 Pct Recovery = 90% Analysis Date = 01/22/16 Pct Recovery = 90% Analysis Date = 01/17/16 Pct Recovery = 90% Analysis Date = 01/17/16 Pct Recovery = 90% Analysis Date = 01/12/16 Pct Recovery = 90% Analysis Date = 01/12/16 Pct Recovery = 90% Analysis Date = 01/08/16 Pct Recovery = 91% Analysis Date = 01/08/16 Pct Recovery = 91% Analysis Date = 01/03/16 Pct Recovery = 91% Analysis Date = 01/03/16 Pct Recovery = 91% Analysis Date = 12/29/15 Pct Recovery = 91% Analysis Date = 12/29/15 Pct Recovery = 91% Analysis Date = 12/25/15 Pct Recovery = 92% Analysis Date = 12/25/15 Pct Recovery = 92% Analysis Date = 12/20/15 Pct Recovery = 92% Analysis Date = 12/20/15 Pct Recovery = 92% Analysis Date = 12/15/15 Pct Recovery = 92% Analysis Date = 12/15/15 Pct Recovery = 92% Analysis Date = 12/10/15 Pct Recovery = 93% Analysis Date = 12/10/15 Pct Recovery = 93% Analysis Date = 12/06/15 Pct Recovery = 93% Analysis Date = 12/06/15 Pct Recovery = 93% Analysis Date = 12/01/15 Pct Recovery = 93% Analysis Date = 12/01/15 Pct Recovery = 93% Analysis Date = 11/26/15 Pct Recovery = 94% Analysis Date = 11/26/15 Pct Recovery = 94% Analysis Date = 11/22/15 Pct Recovery = 94% Analysis Date = 11/22/15 Pct Recovery = 94% Analysis Date = 11/17/15 Pct Recovery = 96% Analysis Date = 11/17/15 Pct Recovery = 96% Analysis Date = 11/12/15 Pct Recovery = 97% Analysis Date = 11/12/15 Pct Recovery = 97% Analysis Date = 11/08/15 Pct Recovery = 98% Analysis Date = 11/08/15 Pct Recovery = 98% Analysis Date = 11/03/15 Pct Recovery = 100% Analysis Date = 11/03/15 Pct Recovery = 100% Analysis Date = 10/29/15 Pct Recovery = 101% Analysis Date = 10/29/15 Pct Recovery = 101% Analysis Date = 10/24/15 Pct Recovery = 102% Analysis Date = 10/24/15 Pct Recovery = 102% Analysis Date = 10/20/15 Pct Recovery = 104% Analysis Date = 10/20/15 Pct Recovery = 104% Analysis Date = 10/15/15 Pct Recovery = 105% Analysis Date = 10/15/15 Pct Recovery = 105% Analysis Date = 10/10/15 Pct Recovery = 106% Analysis Date = 10/10/15 Pct Recovery = 106% Analysis Date = 10/06/15 Pct Recovery = 108% Analysis Date = 10/06/15 Pct Recovery = 108% Analysis Date = 10/01/15 Pct Recovery = 109% Analysis Date = 10/01/15 Pct Recovery = 109% Analysis Date = 09/26/15 Pct Recovery = 110% Analysis Date = 09/26/15 Pct Recovery = 110% Analysis Date = 09/22/15 Pct Recovery = 110% Analysis Date = 09/22/15 Pct Recovery = 110% Analysis Date = 09/17/15 Pct Recovery = 111% Analysis Date = 09/17/15 Pct Recovery = 111% Analysis Date = 09/12/15 Pct Recovery = 111% Analysis Date = 09/12/15 Pct Recovery = 111% Analysis Date = 09/07/15 Pct Recovery = 112% Analysis Date = 09/07/15 Pct Recovery = 112% Analysis Date = 09/03/15 Pct Recovery = 112% Analysis Date = 09/03/15 Pct Recovery = 112% Analysis Date = 08/29/15 Pct Recovery = 113% Analysis Date = 08/29/15 Pct Recovery = 113% Analysis Date = 08/24/15 Pct Recovery = 113% Analysis Date = 08/24/15 Pct Recovery = 113% Analysis Date = 08/20/15 Pct Recovery = 114% Analysis Date = 08/20/15 Pct Recovery = 114% Analysis Date = 08/15/15 Pct Recovery = 114% Analysis Date = 08/15/15 Pct Recovery = 114% Analysis Date = 08/10/15 Pct Recovery = 115% Analysis Date = 08/10/15 Pct Recovery = 115% Analysis Date = 08/06/15 Pct Recovery = 115% Analysis Date = 08/06/15 Pct Recovery = 115% Analysis Date = 08/01/15 Pct Recovery = 116% Analysis Date = 08/01/15 Pct Recovery = 116% Analysis Date = 07/27/15 Pct Recovery = 116% Analysis Date = 07/27/15 Pct Recovery = 116% Analysis Date = 07/22/15 Pct Recovery = 116% Analysis Date = 07/22/15 Pct Recovery = 116% Analysis Date = 07/18/15 Pct Recovery = 116% Analysis Date = 07/18/15 Pct Recovery = 116% Analysis Date = 07/13/15 Pct Recovery = 117% Analysis Date = 07/13/15 Pct Recovery = 117% Analysis Date = 07/08/15 Pct Recovery = 117% Analysis Date = 07/08/15 Pct Recovery = 117% Analysis Date = 07/04/15 Pct Recovery = 117% Analysis Date = 07/04/15 Pct Recovery = 117% Analysis Date = 06/29/15 Pct Recovery = 117% Analysis Date = 06/29/15 Pct Recovery = 117% Analysis Date = 06/24/15 Pct Recovery = 118% Analysis Date = 06/24/15 Pct Recovery = 118% Analysis Date = 06/20/15 Pct Recovery = 118% Analysis Date = 06/20/15 Pct Recovery = 118% Analysis Date = 06/15/15 Pct Recovery = 118% Analysis Date = 06/15/15 Pct Recovery = 118% Analysis Date = 06/10/15 Pct Recovery = 118% Analysis Date = 06/10/15 Pct Recovery = 118% Analysis Date = 06/05/15 Pct Recovery = 119% Analysis Date = 06/05/15 Pct Recovery = 119% Analysis Date = 06/01/15 Pct Recovery = 119% Analysis Date = 06/01/15 Pct Recovery = 119% Analysis Date = 05/27/15 Pct Recovery = 119% Analysis Date = 05/27/15 Pct Recovery = 119% Analysis Date = 05/22/15 Pct Recovery = 119% Analysis Date = 05/22/15 Pct Recovery = 119% Analysis Date = 05/18/15 Pct Recovery = 120% Analysis Date = 05/18/15 Pct Recovery = 120% Analysis Date = 05/13/15 Pct Recovery = 120% Analysis Date = 05/13/15 Pct Recovery = 120% Analysis Date = 05/08/15 Pct Recovery = 120% Analysis Date = 05/08/15 Pct Recovery = 120% Analysis Date = 05/04/15 Pct Recovery = 120% Analysis Date = 05/04/15 Pct Recovery = 120% Analysis Date = 04/29/15 Pct Recovery = 121% Analysis Date = 04/29/15 Pct Recovery = 121% Analysis Date = 04/24/15 Pct Recovery = 121% Analysis Date = 04/24/15 Pct Recovery = 121% Analysis Date = 04/19/15 Pct Recovery = 121% Analysis Date = 04/19/15 Pct Recovery = 121% Analysis Date = 04/15/15 Pct Recovery = 121% Analysis Date = 04/15/15 Pct Recovery = 121% Analysis Date = 04/10/15 Pct Recovery = 121% Analysis Date = 04/10/15 Pct Recovery = 121% Analysis Date = 04/05/15 Pct Recovery = 120% Analysis Date = 04/05/15 Pct Recovery = 120% Analysis Date = 04/01/15 Pct Recovery = 120% Analysis Date = 04/01/15 Pct Recovery = 120% Analysis Date = 03/27/15 Pct Recovery = 120% Analysis Date = 03/27/15 Pct Recovery = 120% Analysis Date = 03/22/15 Pct Recovery = 120% Analysis Date = 03/22/15 Pct Recovery = 120% Analysis Date = 03/18/15 Pct Recovery = 120% Analysis Date = 03/18/15 Pct Recovery = 120% Analysis Date = 03/13/15 Pct Recovery = 120% Analysis Date = 03/13/15 Pct Recovery = 120% Analysis Date = 03/08/15 Pct Recovery = 120% Analysis Date = 03/08/15 Pct Recovery = 120% Analysis Date = 03/03/15 Pct Recovery = 120% Analysis Date = 03/03/15 Pct Recovery = 120% Analysis Date = 02/27/15 Pct Recovery = 120% Analysis Date = 02/27/15 Pct Recovery = 120% Analysis Date = 02/22/15 Pct Recovery = 120% Analysis Date = 02/22/15 Pct Recovery = 120% Analysis Date = 02/17/15 Pct Recovery = 120% Analysis Date = 02/17/15 Pct Recovery = 120% Analysis Date = 02/13/15 Pct Recovery = 120% Analysis Date = 02/13/15 Pct Recovery = 120% Analysis Date = 02/08/15 Pct Recovery = 120% Analysis Date = 02/08/15 Pct Recovery = 120% Analysis Date = 02/03/15 Pct Recovery = 119% Analysis Date = 02/03/15 Pct Recovery = 119% Analysis Date = 01/30/15 Pct Recovery = 118% Analysis Date = 01/30/15 Pct Recovery = 118% Analysis Date = 01/25/15 Pct Recovery = 117% Analysis Date = 01/25/15 Pct Recovery = 117% Analysis Date = 01/20/15 Pct Recovery = 115% Analysis Date = 01/20/15 Pct Recovery = 115% Analysis Date = 01/15/15 Pct Recovery = 114% Analysis Date = 01/15/15 Pct Recovery = 114% Analysis Date = 01/11/15 Pct Recovery = 113% Analysis Date = 01/11/15 Pct Recovery = 113% Analysis Date = 01/06/15 Pct Recovery = 112% Analysis Date = 01/06/15 Pct Recovery = 112% Analysis Date = 01/01/15 Pct Recovery = 110% Analysis Date = 01/01/15 Pct Recovery = 110% Analysis Date = 12/28/14 Pct Recovery = 109% Analysis Date = 12/28/14 Pct Recovery = 109% Analysis Date = 12/23/14 Pct Recovery = 108% Analysis Date = 12/23/14 Pct Recovery = 108% Analysis Date = 12/18/14 Pct Recovery = 107% Analysis Date = 12/18/14 Pct Recovery = 107% Analysis Date = 12/14/14 Pct Recovery = 105% Analysis Date = 12/14/14 Pct Recovery = 105% Analysis Date = 12/09/14 Pct Recovery = 104% Analysis Date = 12/09/14 Pct Recovery = 104% Analysis Date = 12/04/14 Pct Recovery = 103% Analysis Date = 12/04/14 Pct Recovery = 103% Analysis Date = 11/29/14 Pct Recovery = 102% Analysis Date = 11/29/14 Pct Recovery = 102% Analysis Date = 11/25/14 Pct Recovery = 100% Analysis Date = 11/25/14 Pct Recovery = 100% Analysis Date = 11/20/14 Pct Recovery = 99% Analysis Date = 11/20/14 Pct Recovery = 99% Analysis Date = 11/15/14 Pct Recovery = 98% Analysis Date = 11/15/14 Pct Recovery = 98% Analysis Date = 11/11/14 Pct Recovery = 96% Analysis Date = 11/11/14 Pct Recovery = 96% Analysis Date = 11/06/14 Pct Recovery = 95% Analysis Date = 11/06/14 Pct Recovery = 95% Analysis Date = 11/01/14 Pct Recovery = 94% Analysis Date = 11/01/14 Pct Recovery = 94% Analysis Date = 10/28/14 Pct Recovery = 93% Analysis Date = 10/28/14 Pct Recovery = 93% Analysis Date = 10/23/14 Pct Recovery = 91% Analysis Date = 10/23/14 Pct Recovery = 91% Analysis Date = 10/18/14 Pct Recovery = 90% Analysis Date = 10/18/14 Pct Recovery = 90% Analysis Date = 10/13/14 Pct Recovery = 88% Analysis Date = 10/13/14 Pct Recovery = 88% Analysis Date = 10/09/14 Pct Recovery = 87% Analysis Date = 10/09/14 Pct Recovery = 87% Analysis Date = 10/04/14 Pct Recovery = 86% Analysis Date = 10/04/14 Pct Recovery = 86% Analysis Date = 09/29/14 Pct Recovery = 84% Analysis Date = 09/29/14 Pct Recovery = 84% Analysis Date = 09/25/14 Pct Recovery = 83% Analysis Date = 09/25/14 Pct Recovery = 83% Analysis Date = 09/20/14 Pct Recovery = 81% Analysis Date = 09/20/14 Pct Recovery = 81% Analysis Date = 09/15/14 Pct Recovery = 80% Analysis Date = 09/15/14 Pct Recovery = 80% Analysis Date = 09/11/14 Pct Recovery = 79% Analysis Date = 09/11/14 Pct Recovery = 79% Analysis Date = 09/06/14 Pct Recovery = 77% Analysis Date = 09/06/14 Pct Recovery = 77% Analysis Date = 09/01/14 Pct Recovery = 76% Analysis Date = 09/01/14 Pct Recovery = 76% Analysis Date = 08/27/14 Pct Recovery = 74% Analysis Date = 08/27/14 Pct Recovery = 74% Analysis Date = 08/23/14 Pct Recovery = 73% Analysis Date = 08/23/14 Pct Recovery = 73% Analysis Date = 08/18/14 Pct Recovery = 72% Analysis Date = 08/18/14 Pct Recovery = 72% Analysis Date = 08/13/14 Pct Recovery = 70% Analysis Date = 08/13/14 Pct Recovery = 70% Analysis Date = 08/09/14 Pct Recovery = 69% Analysis Date = 08/09/14 Pct Recovery = 69% Analysis Date = 08/04/14 Pct Recovery = 67% Analysis Date = 08/04/14 Pct Recovery = 67% Analysis Date = 07/30/14 Pct Recovery = 66% Analysis Date = 07/30/14 Pct Recovery = 66% Analysis Date = 07/26/14 Pct Recovery = 65% Analysis Date = 07/26/14 Pct Recovery = 65% Analysis Date = 07/21/14 Pct Recovery = 63% Analysis Date = 07/21/14 Pct Recovery = 63% Analysis Date = 07/16/14 Pct Recovery = 62% Analysis Date = 07/16/14 Pct Recovery = 62% Analysis Date = 07/11/14 Pct Recovery = 60% Analysis Date = 07/11/14 Pct Recovery = 60% Analysis Date = 07/07/14 Pct Recovery = 59% Analysis Date = 07/07/14 Pct Recovery = 59% Analysis Date = 07/02/14 Pct Recovery = 58% Analysis Date = 07/02/14 Pct Recovery = 58% Analysis Date = 06/27/14 Pct Recovery = 56% Analysis Date = 06/27/14 Pct Recovery = 56% Analysis Date = 06/23/14 Pct Recovery = 55% Analysis Date = 06/23/14 Pct Recovery = 55% Analysis Date = 06/18/14 Pct Recovery = 54% Analysis Date = 06/18/14 Pct Recovery = 54% Analysis Date = 06/13/14 Pct Recovery = 52% Analysis Date = 06/13/14 Pct Recovery = 52% Analysis Date = 06/09/14 Pct Recovery = 51% Analysis Date = 06/09/14 Pct Recovery = 51% Analysis Date = 06/04/14 Pct Recovery = 50% Analysis Date = 06/04/14 Pct Recovery = 50% Analysis Date = 05/30/14 Pct Recovery = 48% Analysis Date = 05/30/14 Pct Recovery = 48% Analysis Date = 05/25/14 Pct Recovery = 47% Analysis Date = 05/25/14 Pct Recovery = 47% Analysis Date = 05/21/14 Pct Recovery = 46% Analysis Date = 05/21/14 Pct Recovery = 46% Analysis Date = 05/16/14 Pct Recovery = 44% Analysis Date = 05/16/14 Pct Recovery = 44% Analysis Date = 05/11/14 Pct Recovery = 43% Analysis Date = 05/11/14 Pct Recovery = 43% Analysis Date = 05/07/14 Pct Recovery = 42% Analysis Date = 05/07/14 Pct Recovery = 42% Analysis Date = 05/02/14 Pct Recovery = 40% Analysis Date = 05/02/14 Pct Recovery = 40% Analysis Date = 04/27/14 Pct Recovery = 39% Analysis Date = 04/27/14 Pct Recovery = 39% Analysis Date = 04/23/14 Pct Recovery = 38% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
ACETAMINOPHEN

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 3 75% 22% 85% 29%
>= Reporting Level 60 94% 85% 83% 13%
Total 63 93% 83% 84% 13%

Sample Statistics
ACETAMINOPHEN

Characteristic N % % Basis
Plotted 63 83% Spiked
Estimated Values 8 11% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 10 13% Spiked
Spiked 76 .  
False Negatives 3 4% 3 out of 76
Not Spiked 39 .  
False Positives 0 0% 0 out of 39

BQS OBSP Determination:
ACYCLOVIR
METHOD: 2440 , TESTIDCODE: 67484LCM56
Open Data Set

Analysis Date = 10/01/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 231% Analysis Date = 11/05/15 SpikeMix = ERA 0406-15-08: 80 µl & Abs 052215: 80 µl Pct Recovery = 260% Analysis Date = 11/04/15 SpikeMix = Abs 052215: 80 µl & Abs 050115: 80 µl Pct Recovery = 245% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 322% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 342% Analysis Date = 04/29/15 SpikeMix = ERA 0319-14-05: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 432% Analysis Date = 02/06/15 SpikeMix = Abs 041814: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 289% Analysis Date = 07/26/14 SpikeMix = ERA 0319-14-05: 60 µl & ERA 0318-14-02: 60 µl Pct Recovery = 216% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 395% Analysis Date = 12/07/14 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 309% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-08: 40 µl & Abs 052215: 40 µl Pct Recovery = 214% Analysis Date = 02/23/16 SpikeMix = Abs 052215: 40 µl & Abs 050115: 40 µl Pct Recovery = 247% Analysis Date = 07/31/15 SpikeMix = Abs 051315: 40 µl & Abs 052215: 40 µl Pct Recovery = 212% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 327% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 307% Analysis Date = 11/04/14 SpikeMix = Abs 041814: 8 µl & ERA 0318-14-02: 8 µl Pct Recovery = 291% Analysis Date = 10/24/14 SpikeMix = ERA 0319-14-05: 8 µl & Abs 041614: 8 µl Pct Recovery = 343% Analysis Date = 10/10/14 SpikeMix = Abs 041814: 30 µl & ERA 0318-14-02: 30 µl Pct Recovery = 363% Analysis Date = 08/30/14 SpikeMix = ERA 0318-14-02: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 376% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 239% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 255% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 313% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 281% Analysis Date = 08/27/15 SpikeMix = Abs 052215: 20 µl & Abs 050115: 20 µl Pct Recovery = 217% Analysis Date = 07/09/15 SpikeMix = Abs 050115: 20 µl & Abs 052215: 20 µl Pct Recovery = 225% Analysis Date = 06/26/15 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 219% Analysis Date = 04/09/16 SpikeMix = Abs 051315: 10 µl & ERA 0406-15-09: 10 µl Pct Recovery = 336% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 41% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 46% Analysis Date = 01/17/16 SpikeMix = ERA 0406-15-09: 80 µl & ERA 0406-15-07A: 80 µl Pct Recovery = 171% Analysis Date = 11/24/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 126% Analysis Date = 11/18/16 SpikeMix = ERA 04281604: 80 µl & ERA 04281603: 80 µl Pct Recovery = 44% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & ERA 04281604: 80 µl Pct Recovery = 46% Analysis Date = 03/11/15 SpikeMix = ERA 0318-14-02: 15 µl & Abs 041714: 15 µl Pct Recovery = 89% Analysis Date = 12/06/14 SpikeMix = ERA 0318-14-02: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 63% Analysis Date = 10/11/14 SpikeMix = ERA 0318-14-02: 60 µl & ERA 0319-14-04: 60 µl Pct Recovery = 60% Analysis Date = 08/21/14 SpikeMix = ERA 0318-14-02: 60 µl & Abs 041714: 60 µl Pct Recovery = 25% Analysis Date = 10/25/14 SpikeMix = Abs 041614: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 62% Analysis Date = 06/22/14 SpikeMix = Abs 041814: 60 µl & Abs 041614: 60 µl Pct Recovery = 142% Analysis Date = 06/11/14 SpikeMix = Abs 041614: 60 µl & Abs 041714: 60 µl Pct Recovery = 22% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-08: 40 µl & ERA 0406-15-09: 40 µl Pct Recovery = 187% Analysis Date = 07/31/15 SpikeMix = ERA 0406-15-09: 40 µl & Abs 050115: 40 µl Pct Recovery = 153% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 166% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 170% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 111% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 104% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 57% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 48% Analysis Date = 12/07/14 SpikeMix = ERA 0318-14-02: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 68% Analysis Date = 04/30/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 74% Analysis Date = 02/10/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 66% Analysis Date = 07/20/14 SpikeMix = ERA 0318-14-02: 30 µl & Abs 041714: 30 µl Pct Recovery = 34% Analysis Date = 09/12/14 SpikeMix = Abs 041614: 30 µl & ERA 0319-14-04: 30 µl Pct Recovery = 47% Analysis Date = 07/13/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 134% Analysis Date = 06/28/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 20% Analysis Date = 05/30/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 114% Analysis Date = 05/17/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 28% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-08: 20 µl & ERA 0406-15-09: 20 µl Pct Recovery = 102% Analysis Date = 11/24/15 SpikeMix = ERA 0406-15-09: 20 µl & Abs 050115: 20 µl Pct Recovery = 191% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-09: 20 µl Pct Recovery = 150% Analysis Date = 11/24/15 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 141% Analysis Date = 01/04/17 Pct Recovery = 108% Analysis Date = 12/31/16 Pct Recovery = 111% Analysis Date = 12/31/16 Pct Recovery = 111% Analysis Date = 12/26/16 Pct Recovery = 113% Analysis Date = 12/26/16 Pct Recovery = 113% Analysis Date = 12/21/16 Pct Recovery = 115% Analysis Date = 12/21/16 Pct Recovery = 115% Analysis Date = 12/16/16 Pct Recovery = 118% Analysis Date = 12/16/16 Pct Recovery = 118% Analysis Date = 12/11/16 Pct Recovery = 120% Analysis Date = 12/11/16 Pct Recovery = 120% Analysis Date = 12/07/16 Pct Recovery = 122% Analysis Date = 12/07/16 Pct Recovery = 122% Analysis Date = 12/02/16 Pct Recovery = 125% Analysis Date = 12/02/16 Pct Recovery = 125% Analysis Date = 11/27/16 Pct Recovery = 127% Analysis Date = 11/27/16 Pct Recovery = 127% Analysis Date = 11/22/16 Pct Recovery = 130% Analysis Date = 11/22/16 Pct Recovery = 130% Analysis Date = 11/17/16 Pct Recovery = 132% Analysis Date = 11/17/16 Pct Recovery = 132% Analysis Date = 11/12/16 Pct Recovery = 134% Analysis Date = 11/12/16 Pct Recovery = 134% Analysis Date = 11/08/16 Pct Recovery = 137% Analysis Date = 11/08/16 Pct Recovery = 137% Analysis Date = 11/03/16 Pct Recovery = 139% Analysis Date = 11/03/16 Pct Recovery = 139% Analysis Date = 10/29/16 Pct Recovery = 142% Analysis Date = 10/29/16 Pct Recovery = 142% Analysis Date = 10/24/16 Pct Recovery = 144% Analysis Date = 10/24/16 Pct Recovery = 144% Analysis Date = 10/19/16 Pct Recovery = 146% Analysis Date = 10/19/16 Pct Recovery = 146% Analysis Date = 10/15/16 Pct Recovery = 148% Analysis Date = 10/15/16 Pct Recovery = 148% Analysis Date = 10/10/16 Pct Recovery = 150% Analysis Date = 10/10/16 Pct Recovery = 150% Analysis Date = 10/05/16 Pct Recovery = 152% Analysis Date = 10/05/16 Pct Recovery = 152% Analysis Date = 09/30/16 Pct Recovery = 154% Analysis Date = 09/30/16 Pct Recovery = 154% Analysis Date = 09/25/16 Pct Recovery = 156% Analysis Date = 09/25/16 Pct Recovery = 156% Analysis Date = 09/20/16 Pct Recovery = 158% Analysis Date = 09/20/16 Pct Recovery = 158% Analysis Date = 09/16/16 Pct Recovery = 159% Analysis Date = 09/16/16 Pct Recovery = 159% Analysis Date = 09/11/16 Pct Recovery = 161% Analysis Date = 09/11/16 Pct Recovery = 161% Analysis Date = 09/06/16 Pct Recovery = 163% Analysis Date = 09/06/16 Pct Recovery = 163% Analysis Date = 09/01/16 Pct Recovery = 165% Analysis Date = 09/01/16 Pct Recovery = 165% Analysis Date = 08/27/16 Pct Recovery = 167% Analysis Date = 08/27/16 Pct Recovery = 167% Analysis Date = 08/23/16 Pct Recovery = 169% Analysis Date = 08/23/16 Pct Recovery = 169% Analysis Date = 08/18/16 Pct Recovery = 171% Analysis Date = 08/18/16 Pct Recovery = 171% Analysis Date = 08/13/16 Pct Recovery = 173% Analysis Date = 08/13/16 Pct Recovery = 173% Analysis Date = 08/08/16 Pct Recovery = 175% Analysis Date = 08/08/16 Pct Recovery = 175% Analysis Date = 08/03/16 Pct Recovery = 177% Analysis Date = 08/03/16 Pct Recovery = 177% Analysis Date = 07/29/16 Pct Recovery = 179% Analysis Date = 07/29/16 Pct Recovery = 179% Analysis Date = 07/25/16 Pct Recovery = 180% Analysis Date = 07/25/16 Pct Recovery = 180% Analysis Date = 07/20/16 Pct Recovery = 182% Analysis Date = 07/20/16 Pct Recovery = 182% Analysis Date = 07/15/16 Pct Recovery = 184% Analysis Date = 07/15/16 Pct Recovery = 184% Analysis Date = 07/10/16 Pct Recovery = 186% Analysis Date = 07/10/16 Pct Recovery = 186% Analysis Date = 07/05/16 Pct Recovery = 188% Analysis Date = 07/05/16 Pct Recovery = 188% Analysis Date = 07/01/16 Pct Recovery = 189% Analysis Date = 07/01/16 Pct Recovery = 189% Analysis Date = 06/26/16 Pct Recovery = 191% Analysis Date = 06/26/16 Pct Recovery = 191% Analysis Date = 06/21/16 Pct Recovery = 193% Analysis Date = 06/21/16 Pct Recovery = 193% Analysis Date = 06/16/16 Pct Recovery = 195% Analysis Date = 06/16/16 Pct Recovery = 195% Analysis Date = 06/11/16 Pct Recovery = 197% Analysis Date = 06/11/16 Pct Recovery = 197% Analysis Date = 06/06/16 Pct Recovery = 198% Analysis Date = 06/06/16 Pct Recovery = 198% Analysis Date = 06/02/16 Pct Recovery = 200% Analysis Date = 06/02/16 Pct Recovery = 200% Analysis Date = 05/28/16 Pct Recovery = 202% Analysis Date = 05/28/16 Pct Recovery = 202% Analysis Date = 05/23/16 Pct Recovery = 204% Analysis Date = 05/23/16 Pct Recovery = 204% Analysis Date = 06/16/15 Pct Recovery = 204% Analysis Date = 06/16/15 Pct Recovery = 204% Analysis Date = 06/11/15 Pct Recovery = 204% Analysis Date = 06/11/15 Pct Recovery = 204% Analysis Date = 06/06/15 Pct Recovery = 204% Analysis Date = 06/06/15 Pct Recovery = 204% Analysis Date = 06/01/15 Pct Recovery = 204% Analysis Date = 06/01/15 Pct Recovery = 204% Analysis Date = 05/27/15 Pct Recovery = 204% Analysis Date = 05/27/15 Pct Recovery = 204% Analysis Date = 05/23/15 Pct Recovery = 204% Analysis Date = 05/23/15 Pct Recovery = 204% Analysis Date = 05/18/15 Pct Recovery = 204% Analysis Date = 05/18/15 Pct Recovery = 204% Analysis Date = 05/13/15 Pct Recovery = 203% Analysis Date = 05/13/15 Pct Recovery = 203% Analysis Date = 05/08/15 Pct Recovery = 203% Analysis Date = 05/08/15 Pct Recovery = 203% Analysis Date = 05/03/15 Pct Recovery = 203% Analysis Date = 05/03/15 Pct Recovery = 203% Analysis Date = 04/29/15 Pct Recovery = 203% Analysis Date = 04/29/15 Pct Recovery = 203% Analysis Date = 04/24/15 Pct Recovery = 203% Analysis Date = 04/24/15 Pct Recovery = 203% Analysis Date = 04/19/15 Pct Recovery = 203% Analysis Date = 04/19/15 Pct Recovery = 203% Analysis Date = 04/14/15 Pct Recovery = 202% Analysis Date = 04/14/15 Pct Recovery = 202% Analysis Date = 04/09/15 Pct Recovery = 202% Analysis Date = 04/09/15 Pct Recovery = 202% Analysis Date = 04/04/15 Pct Recovery = 202% Analysis Date = 04/04/15 Pct Recovery = 202% Analysis Date = 03/31/15 Pct Recovery = 202% Analysis Date = 03/31/15 Pct Recovery = 202% Analysis Date = 03/26/15 Pct Recovery = 201% Analysis Date = 03/26/15 Pct Recovery = 201% Analysis Date = 03/21/15 Pct Recovery = 201% Analysis Date = 03/21/15 Pct Recovery = 201% Analysis Date = 03/16/15 Pct Recovery = 201% Analysis Date = 03/16/15 Pct Recovery = 201% Analysis Date = 03/11/15 Pct Recovery = 201% Analysis Date = 03/11/15 Pct Recovery = 201% Analysis Date = 03/07/15 Pct Recovery = 200% Analysis Date = 03/07/15 Pct Recovery = 200% Analysis Date = 03/02/15 Pct Recovery = 200% Analysis Date = 03/02/15 Pct Recovery = 200% Analysis Date = 02/25/15 Pct Recovery = 200% Analysis Date = 02/25/15 Pct Recovery = 200% Analysis Date = 02/20/15 Pct Recovery = 200% Analysis Date = 02/20/15 Pct Recovery = 200% Analysis Date = 02/15/15 Pct Recovery = 200% Analysis Date = 02/15/15 Pct Recovery = 200% Analysis Date = 02/10/15 Pct Recovery = 199% Analysis Date = 02/10/15 Pct Recovery = 199% Analysis Date = 02/06/15 Pct Recovery = 199% Analysis Date = 02/06/15 Pct Recovery = 199% Analysis Date = 02/01/15 Pct Recovery = 197% Analysis Date = 02/01/15 Pct Recovery = 197% Analysis Date = 01/27/15 Pct Recovery = 196% Analysis Date = 01/27/15 Pct Recovery = 196% Analysis Date = 01/22/15 Pct Recovery = 194% Analysis Date = 01/22/15 Pct Recovery = 194% Analysis Date = 01/17/15 Pct Recovery = 192% Analysis Date = 01/17/15 Pct Recovery = 192% Analysis Date = 01/12/15 Pct Recovery = 191% Analysis Date = 01/12/15 Pct Recovery = 191% Analysis Date = 01/08/15 Pct Recovery = 189% Analysis Date = 01/08/15 Pct Recovery = 189% Analysis Date = 01/03/15 Pct Recovery = 187% Analysis Date = 01/03/15 Pct Recovery = 187% Analysis Date = 12/29/14 Pct Recovery = 185% Analysis Date = 12/29/14 Pct Recovery = 185% Analysis Date = 12/24/14 Pct Recovery = 184% Analysis Date = 12/24/14 Pct Recovery = 184% Analysis Date = 12/19/14 Pct Recovery = 182% Analysis Date = 12/19/14 Pct Recovery = 182% Analysis Date = 12/15/14 Pct Recovery = 180% Analysis Date = 12/15/14 Pct Recovery = 180% Analysis Date = 12/10/14 Pct Recovery = 179% Analysis Date = 12/10/14 Pct Recovery = 179% Analysis Date = 12/05/14 Pct Recovery = 177% Analysis Date = 12/05/14 Pct Recovery = 177% Analysis Date = 11/30/14 Pct Recovery = 175% Analysis Date = 11/30/14 Pct Recovery = 175% Analysis Date = 11/25/14 Pct Recovery = 174% Analysis Date = 11/25/14 Pct Recovery = 174% Analysis Date = 11/20/14 Pct Recovery = 172% Analysis Date = 11/20/14 Pct Recovery = 172% Analysis Date = 11/16/14 Pct Recovery = 170% Analysis Date = 11/16/14 Pct Recovery = 170% Analysis Date = 11/11/14 Pct Recovery = 168% Analysis Date = 11/11/14 Pct Recovery = 168% Analysis Date = 11/06/14 Pct Recovery = 167% Analysis Date = 11/06/14 Pct Recovery = 167% Analysis Date = 11/01/14 Pct Recovery = 165% Analysis Date = 11/01/14 Pct Recovery = 165% Analysis Date = 10/27/14 Pct Recovery = 163% Analysis Date = 10/27/14 Pct Recovery = 163% Analysis Date = 10/23/14 Pct Recovery = 161% Analysis Date = 10/23/14 Pct Recovery = 161% Analysis Date = 10/18/14 Pct Recovery = 159% Analysis Date = 10/18/14 Pct Recovery = 159% Analysis Date = 10/13/14 Pct Recovery = 157% Analysis Date = 10/13/14 Pct Recovery = 157% Analysis Date = 10/08/14 Pct Recovery = 155% Analysis Date = 10/08/14 Pct Recovery = 155% Analysis Date = 10/03/14 Pct Recovery = 153% Analysis Date = 10/03/14 Pct Recovery = 153% Analysis Date = 09/28/14 Pct Recovery = 151% Analysis Date = 09/28/14 Pct Recovery = 151% Analysis Date = 09/24/14 Pct Recovery = 149% Analysis Date = 09/24/14 Pct Recovery = 149% Analysis Date = 09/19/14 Pct Recovery = 147% Analysis Date = 09/19/14 Pct Recovery = 147% Analysis Date = 09/14/14 Pct Recovery = 145% Analysis Date = 09/14/14 Pct Recovery = 145% Analysis Date = 09/09/14 Pct Recovery = 143% Analysis Date = 09/09/14 Pct Recovery = 143% Analysis Date = 09/04/14 Pct Recovery = 141% Analysis Date = 09/04/14 Pct Recovery = 141% Analysis Date = 08/31/14 Pct Recovery = 139% Analysis Date = 08/31/14 Pct Recovery = 139% Analysis Date = 08/26/14 Pct Recovery = 137% Analysis Date = 08/26/14 Pct Recovery = 137% Analysis Date = 08/21/14 Pct Recovery = 135% Analysis Date = 08/21/14 Pct Recovery = 135% Analysis Date = 08/16/14 Pct Recovery = 133% Analysis Date = 08/16/14 Pct Recovery = 133% Analysis Date = 08/11/14 Pct Recovery = 131% Analysis Date = 08/11/14 Pct Recovery = 131% Analysis Date = 08/06/14 Pct Recovery = 129% Analysis Date = 08/06/14 Pct Recovery = 129% Analysis Date = 08/02/14 Pct Recovery = 127% Analysis Date = 08/02/14 Pct Recovery = 127% Analysis Date = 07/28/14 Pct Recovery = 125% Analysis Date = 07/28/14 Pct Recovery = 125% Analysis Date = 07/23/14 Pct Recovery = 123% Analysis Date = 07/23/14 Pct Recovery = 123% Analysis Date = 07/18/14 Pct Recovery = 121% Analysis Date = 07/18/14 Pct Recovery = 121% Analysis Date = 07/13/14 Pct Recovery = 119% Analysis Date = 07/13/14 Pct Recovery = 119% Analysis Date = 07/09/14 Pct Recovery = 117% Analysis Date = 07/09/14 Pct Recovery = 117% Analysis Date = 07/04/14 Pct Recovery = 114% Analysis Date = 07/04/14 Pct Recovery = 114% Analysis Date = 06/29/14 Pct Recovery = 112% Analysis Date = 06/29/14 Pct Recovery = 112% Analysis Date = 06/24/14 Pct Recovery = 110% Analysis Date = 06/24/14 Pct Recovery = 110% Analysis Date = 06/19/14 Pct Recovery = 108% Analysis Date = 06/19/14 Pct Recovery = 108% Analysis Date = 06/14/14 Pct Recovery = 106% Analysis Date = 06/14/14 Pct Recovery = 106% Analysis Date = 06/10/14 Pct Recovery = 103% Analysis Date = 06/10/14 Pct Recovery = 103% Analysis Date = 06/05/14 Pct Recovery = 101% Analysis Date = 06/05/14 Pct Recovery = 101% Analysis Date = 05/31/14 Pct Recovery = 99% Analysis Date = 05/31/14 Pct Recovery = 99% Analysis Date = 05/26/14 Pct Recovery = 97% Analysis Date = 05/26/14 Pct Recovery = 97% Analysis Date = 05/21/14 Pct Recovery = 94% Analysis Date = 05/21/14 Pct Recovery = 94% Analysis Date = 05/17/14 Pct Recovery = 92% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
ACYCLOVIR

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 1 336% . 336% 0%
>= Reporting Level 60 176% 113% 168% 143%
Total 61 179% 114% 170% 144%

Sample Statistics
ACYCLOVIR

Characteristic N % % Basis
Plotted 61 81% Spiked
Estimated Values 10 13% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 4 5% Spiked
Spiked 75 .  
False Negatives 10 13% 10 out of 75
Not Spiked 40 .  
False Positives 21 53% 21 out of 40

BQS OBSP Determination:
ALBUTEROL (SALBUTAMOL)
METHOD: 2440 , TESTIDCODE: 67437LCM56
Open Data Set

Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 96% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 96% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 76% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 75% Analysis Date = 01/17/16 SpikeMix = ERA 0406-15-09: 80 µl & ERA 0406-15-07A: 80 µl Pct Recovery = 82% Analysis Date = 11/24/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 77% Analysis Date = 10/01/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 52% Analysis Date = 11/05/15 SpikeMix = ERA 0406-15-08: 80 µl & Abs 052215: 80 µl Pct Recovery = 76% Analysis Date = 11/04/15 SpikeMix = Abs 052215: 80 µl & Abs 050115: 80 µl Pct Recovery = 81% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 74% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 79% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 83% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 84% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 67% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 69% Analysis Date = 09/24/16 SpikeMix = Crescent EN160610015: 80 µl & Abs 061416: 80 µl Pct Recovery = 65% Analysis Date = 09/24/16 SpikeMix = Abs 061416: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 62% Analysis Date = 04/29/15 SpikeMix = ERA 0319-14-05: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 106% Analysis Date = 03/11/15 SpikeMix = ERA 0318-14-02: 15 µl & Abs 041714: 15 µl Pct Recovery = 88% Analysis Date = 02/06/15 SpikeMix = Abs 041814: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 86% Analysis Date = 12/06/14 SpikeMix = ERA 0318-14-02: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 63% Analysis Date = 10/11/14 SpikeMix = ERA 0318-14-02: 60 µl & ERA 0319-14-04: 60 µl Pct Recovery = 59% Analysis Date = 08/21/14 SpikeMix = ERA 0318-14-02: 60 µl & Abs 041714: 60 µl Pct Recovery = 59% Analysis Date = 07/26/14 SpikeMix = ERA 0319-14-05: 60 µl & ERA 0318-14-02: 60 µl Pct Recovery = 65% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 91% Analysis Date = 12/07/14 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 72% Analysis Date = 10/25/14 SpikeMix = Abs 041614: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 72% Analysis Date = 06/22/14 SpikeMix = Abs 041814: 60 µl & Abs 041614: 60 µl Pct Recovery = 89% Analysis Date = 06/11/14 SpikeMix = Abs 041614: 60 µl & Abs 041714: 60 µl Pct Recovery = 79% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-08: 40 µl & ERA 0406-15-09: 40 µl Pct Recovery = 75% Analysis Date = 07/31/15 SpikeMix = ERA 0406-15-09: 40 µl & Abs 050115: 40 µl Pct Recovery = 99% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-08: 40 µl & Abs 052215: 40 µl Pct Recovery = 68% Analysis Date = 02/23/16 SpikeMix = Abs 052215: 40 µl & Abs 050115: 40 µl Pct Recovery = 95% Analysis Date = 09/10/15 SpikeMix = Abs 052215: 40 µl & ERA 0406-15-07A: 40 µl Pct Recovery = 88% Analysis Date = 07/31/15 SpikeMix = Abs 051315: 40 µl & Abs 052215: 40 µl Pct Recovery = 87% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 65% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 65% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 75% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 69% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 84% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 96% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 75% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 64% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 80% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 76% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 71% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 70% Analysis Date = 12/07/14 SpikeMix = ERA 0318-14-02: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 67% Analysis Date = 11/04/14 SpikeMix = Abs 041814: 8 µl & ERA 0318-14-02: 8 µl Pct Recovery = 82% Analysis Date = 04/30/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 104% Analysis Date = 02/10/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 82% Analysis Date = 10/24/14 SpikeMix = ERA 0319-14-05: 8 µl & Abs 041614: 8 µl Pct Recovery = 84% Analysis Date = 10/10/14 SpikeMix = Abs 041814: 30 µl & ERA 0318-14-02: 30 µl Pct Recovery = 43% Analysis Date = 08/30/14 SpikeMix = ERA 0318-14-02: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 84% Analysis Date = 07/20/14 SpikeMix = ERA 0318-14-02: 30 µl & Abs 041714: 30 µl Pct Recovery = 59% Analysis Date = 09/12/14 SpikeMix = Abs 041614: 30 µl & ERA 0319-14-04: 30 µl Pct Recovery = 24% Analysis Date = 07/13/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 63% Analysis Date = 06/28/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 81% Analysis Date = 05/30/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 79% Analysis Date = 05/17/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 87% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 91% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 72% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-08: 20 µl & ERA 0406-15-09: 20 µl Pct Recovery = 64% Analysis Date = 11/24/15 SpikeMix = ERA 0406-15-09: 20 µl & Abs 050115: 20 µl Pct Recovery = 77% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-09: 20 µl Pct Recovery = 40% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 82% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 85% Analysis Date = 02/23/16 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 112% Analysis Date = 11/24/15 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 82% Analysis Date = 09/09/15 SpikeMix = ERA 0406-15-08: 20 µl & Abs 052215: 20 µl Pct Recovery = 80% Analysis Date = 08/27/15 SpikeMix = Abs 052215: 20 µl & Abs 050115: 20 µl Pct Recovery = 65% Analysis Date = 07/09/15 SpikeMix = Abs 050115: 20 µl & Abs 052215: 20 µl Pct Recovery = 105% Analysis Date = 06/26/15 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 72% Analysis Date = 04/23/14 SpikeMix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.2: 20 µl Pct Recovery = 60% Analysis Date = 04/09/16 SpikeMix = Abs 051315: 10 µl & ERA 0406-15-09: 10 µl Pct Recovery = 87% Analysis Date = 01/18/17 Pct Recovery = 74% Analysis Date = 01/13/17 Pct Recovery = 75% Analysis Date = 01/13/17 Pct Recovery = 75% Analysis Date = 01/08/17 Pct Recovery = 75% Analysis Date = 01/08/17 Pct Recovery = 75% Analysis Date = 01/03/17 Pct Recovery = 75% Analysis Date = 01/03/17 Pct Recovery = 75% Analysis Date = 12/29/16 Pct Recovery = 75% Analysis Date = 12/29/16 Pct Recovery = 75% Analysis Date = 12/24/16 Pct Recovery = 75% Analysis Date = 12/24/16 Pct Recovery = 75% Analysis Date = 12/19/16 Pct Recovery = 75% Analysis Date = 12/19/16 Pct Recovery = 75% Analysis Date = 12/14/16 Pct Recovery = 75% Analysis Date = 12/14/16 Pct Recovery = 75% Analysis Date = 12/09/16 Pct Recovery = 75% Analysis Date = 12/09/16 Pct Recovery = 75% Analysis Date = 12/04/16 Pct Recovery = 75% Analysis Date = 12/04/16 Pct Recovery = 75% Analysis Date = 11/29/16 Pct Recovery = 75% Analysis Date = 11/29/16 Pct Recovery = 75% Analysis Date = 11/24/16 Pct Recovery = 76% Analysis Date = 11/24/16 Pct Recovery = 76% Analysis Date = 11/19/16 Pct Recovery = 76% Analysis Date = 11/19/16 Pct Recovery = 76% Analysis Date = 11/14/16 Pct Recovery = 76% Analysis Date = 11/14/16 Pct Recovery = 76% Analysis Date = 11/09/16 Pct Recovery = 76% Analysis Date = 11/09/16 Pct Recovery = 76% Analysis Date = 11/04/16 Pct Recovery = 76% Analysis Date = 11/04/16 Pct Recovery = 76% Analysis Date = 10/30/16 Pct Recovery = 76% Analysis Date = 10/30/16 Pct Recovery = 76% Analysis Date = 10/25/16 Pct Recovery = 76% Analysis Date = 10/25/16 Pct Recovery = 76% Analysis Date = 10/20/16 Pct Recovery = 76% Analysis Date = 10/20/16 Pct Recovery = 76% Analysis Date = 10/15/16 Pct Recovery = 76% Analysis Date = 10/15/16 Pct Recovery = 76% Analysis Date = 10/10/16 Pct Recovery = 76% Analysis Date = 10/10/16 Pct Recovery = 76% Analysis Date = 10/05/16 Pct Recovery = 76% Analysis Date = 10/05/16 Pct Recovery = 76% Analysis Date = 09/30/16 Pct Recovery = 77% Analysis Date = 09/30/16 Pct Recovery = 77% Analysis Date = 09/25/16 Pct Recovery = 77% Analysis Date = 09/25/16 Pct Recovery = 77% Analysis Date = 09/20/16 Pct Recovery = 77% Analysis Date = 09/20/16 Pct Recovery = 77% Analysis Date = 09/15/16 Pct Recovery = 77% Analysis Date = 09/15/16 Pct Recovery = 77% Analysis Date = 09/10/16 Pct Recovery = 77% Analysis Date = 09/10/16 Pct Recovery = 77% Analysis Date = 09/05/16 Pct Recovery = 77% Analysis Date = 09/05/16 Pct Recovery = 77% Analysis Date = 08/31/16 Pct Recovery = 77% Analysis Date = 08/31/16 Pct Recovery = 77% Analysis Date = 08/26/16 Pct Recovery = 77% Analysis Date = 08/26/16 Pct Recovery = 77% Analysis Date = 08/21/16 Pct Recovery = 77% Analysis Date = 08/21/16 Pct Recovery = 77% Analysis Date = 08/16/16 Pct Recovery = 77% Analysis Date = 08/16/16 Pct Recovery = 77% Analysis Date = 08/11/16 Pct Recovery = 78% Analysis Date = 08/11/16 Pct Recovery = 78% Analysis Date = 08/06/16 Pct Recovery = 78% Analysis Date = 08/06/16 Pct Recovery = 78% Analysis Date = 08/01/16 Pct Recovery = 78% Analysis Date = 08/01/16 Pct Recovery = 78% Analysis Date = 07/27/16 Pct Recovery = 78% Analysis Date = 07/27/16 Pct Recovery = 78% Analysis Date = 07/22/16 Pct Recovery = 78% Analysis Date = 07/22/16 Pct Recovery = 78% Analysis Date = 07/17/16 Pct Recovery = 78% Analysis Date = 07/17/16 Pct Recovery = 78% Analysis Date = 07/12/16 Pct Recovery = 78% Analysis Date = 07/12/16 Pct Recovery = 78% Analysis Date = 07/07/16 Pct Recovery = 78% Analysis Date = 07/07/16 Pct Recovery = 78% Analysis Date = 07/02/16 Pct Recovery = 78% Analysis Date = 07/02/16 Pct Recovery = 78% Analysis Date = 06/27/16 Pct Recovery = 78% Analysis Date = 06/27/16 Pct Recovery = 78% Analysis Date = 06/22/16 Pct Recovery = 78% Analysis Date = 06/22/16 Pct Recovery = 78% Analysis Date = 06/17/16 Pct Recovery = 79% Analysis Date = 06/17/16 Pct Recovery = 79% Analysis Date = 06/12/16 Pct Recovery = 79% Analysis Date = 06/12/16 Pct Recovery = 79% Analysis Date = 06/07/16 Pct Recovery = 79% Analysis Date = 06/07/16 Pct Recovery = 79% Analysis Date = 06/02/16 Pct Recovery = 79% Analysis Date = 06/02/16 Pct Recovery = 79% Analysis Date = 05/28/16 Pct Recovery = 79% Analysis Date = 05/28/16 Pct Recovery = 79% Analysis Date = 05/23/16 Pct Recovery = 79% Analysis Date = 05/23/16 Pct Recovery = 79% Analysis Date = 05/18/16 Pct Recovery = 79% Analysis Date = 05/18/16 Pct Recovery = 79% Analysis Date = 05/13/16 Pct Recovery = 79% Analysis Date = 05/13/16 Pct Recovery = 79% Analysis Date = 05/08/16 Pct Recovery = 79% Analysis Date = 05/08/16 Pct Recovery = 79% Analysis Date = 05/03/16 Pct Recovery = 79% Analysis Date = 05/03/16 Pct Recovery = 79% Analysis Date = 04/28/16 Pct Recovery = 80% Analysis Date = 04/28/16 Pct Recovery = 80% Analysis Date = 04/23/16 Pct Recovery = 80% Analysis Date = 04/23/16 Pct Recovery = 80% Analysis Date = 04/18/16 Pct Recovery = 80% Analysis Date = 04/18/16 Pct Recovery = 80% Analysis Date = 04/13/16 Pct Recovery = 80% Analysis Date = 04/13/16 Pct Recovery = 80% Analysis Date = 04/08/16 Pct Recovery = 80% Analysis Date = 04/08/16 Pct Recovery = 80% Analysis Date = 04/03/16 Pct Recovery = 80% Analysis Date = 04/03/16 Pct Recovery = 80% Analysis Date = 03/29/16 Pct Recovery = 80% Analysis Date = 03/29/16 Pct Recovery = 80% Analysis Date = 03/24/16 Pct Recovery = 80% Analysis Date = 03/24/16 Pct Recovery = 80% Analysis Date = 03/19/16 Pct Recovery = 80% Analysis Date = 03/19/16 Pct Recovery = 80% Analysis Date = 03/14/16 Pct Recovery = 80% Analysis Date = 03/14/16 Pct Recovery = 80% Analysis Date = 03/09/16 Pct Recovery = 80% Analysis Date = 03/09/16 Pct Recovery = 80% Analysis Date = 03/04/16 Pct Recovery = 80% Analysis Date = 03/04/16 Pct Recovery = 80% Analysis Date = 02/28/16 Pct Recovery = 80% Analysis Date = 02/28/16 Pct Recovery = 80% Analysis Date = 02/23/16 Pct Recovery = 80% Analysis Date = 02/23/16 Pct Recovery = 80% Analysis Date = 02/18/16 Pct Recovery = 80% Analysis Date = 02/18/16 Pct Recovery = 80% Analysis Date = 02/13/16 Pct Recovery = 80% Analysis Date = 02/13/16 Pct Recovery = 80% Analysis Date = 02/08/16 Pct Recovery = 80% Analysis Date = 02/08/16 Pct Recovery = 80% Analysis Date = 02/03/16 Pct Recovery = 80% Analysis Date = 02/03/16 Pct Recovery = 80% Analysis Date = 01/29/16 Pct Recovery = 79% Analysis Date = 01/29/16 Pct Recovery = 79% Analysis Date = 01/24/16 Pct Recovery = 79% Analysis Date = 01/24/16 Pct Recovery = 79% Analysis Date = 01/19/16 Pct Recovery = 79% Analysis Date = 01/19/16 Pct Recovery = 79% Analysis Date = 01/14/16 Pct Recovery = 79% Analysis Date = 01/14/16 Pct Recovery = 79% Analysis Date = 01/09/16 Pct Recovery = 80% Analysis Date = 01/09/16 Pct Recovery = 80% Analysis Date = 01/04/16 Pct Recovery = 80% Analysis Date = 01/04/16 Pct Recovery = 80% Analysis Date = 12/30/15 Pct Recovery = 80% Analysis Date = 12/30/15 Pct Recovery = 80% Analysis Date = 12/25/15 Pct Recovery = 80% Analysis Date = 12/25/15 Pct Recovery = 80% Analysis Date = 12/20/15 Pct Recovery = 80% Analysis Date = 12/20/15 Pct Recovery = 80% Analysis Date = 12/15/15 Pct Recovery = 80% Analysis Date = 12/15/15 Pct Recovery = 80% Analysis Date = 12/10/15 Pct Recovery = 80% Analysis Date = 12/10/15 Pct Recovery = 80% Analysis Date = 12/05/15 Pct Recovery = 80% Analysis Date = 12/05/15 Pct Recovery = 80% Analysis Date = 11/30/15 Pct Recovery = 80% Analysis Date = 11/30/15 Pct Recovery = 80% Analysis Date = 11/25/15 Pct Recovery = 80% Analysis Date = 11/25/15 Pct Recovery = 80% Analysis Date = 11/20/15 Pct Recovery = 80% Analysis Date = 11/20/15 Pct Recovery = 80% Analysis Date = 11/15/15 Pct Recovery = 80% Analysis Date = 11/15/15 Pct Recovery = 80% Analysis Date = 11/10/15 Pct Recovery = 80% Analysis Date = 11/10/15 Pct Recovery = 80% Analysis Date = 11/05/15 Pct Recovery = 80% Analysis Date = 11/05/15 Pct Recovery = 80% Analysis Date = 10/31/15 Pct Recovery = 80% Analysis Date = 10/31/15 Pct Recovery = 80% Analysis Date = 10/26/15 Pct Recovery = 80% Analysis Date = 10/26/15 Pct Recovery = 80% Analysis Date = 10/21/15 Pct Recovery = 80% Analysis Date = 10/21/15 Pct Recovery = 80% Analysis Date = 10/16/15 Pct Recovery = 81% Analysis Date = 10/16/15 Pct Recovery = 81% Analysis Date = 10/11/15 Pct Recovery = 81% Analysis Date = 10/11/15 Pct Recovery = 81% Analysis Date = 10/06/15 Pct Recovery = 81% Analysis Date = 10/06/15 Pct Recovery = 81% Analysis Date = 10/01/15 Pct Recovery = 81% Analysis Date = 10/01/15 Pct Recovery = 81% Analysis Date = 09/26/15 Pct Recovery = 81% Analysis Date = 09/26/15 Pct Recovery = 81% Analysis Date = 09/21/15 Pct Recovery = 81% Analysis Date = 09/21/15 Pct Recovery = 81% Analysis Date = 09/16/15 Pct Recovery = 81% Analysis Date = 09/16/15 Pct Recovery = 81% Analysis Date = 09/11/15 Pct Recovery = 81% Analysis Date = 09/11/15 Pct Recovery = 81% Analysis Date = 09/05/15 Pct Recovery = 81% Analysis Date = 09/05/15 Pct Recovery = 81% Analysis Date = 08/31/15 Pct Recovery = 81% Analysis Date = 08/31/15 Pct Recovery = 81% Analysis Date = 08/26/15 Pct Recovery = 81% Analysis Date = 08/26/15 Pct Recovery = 81% Analysis Date = 08/21/15 Pct Recovery = 81% Analysis Date = 08/21/15 Pct Recovery = 81% Analysis Date = 08/16/15 Pct Recovery = 81% Analysis Date = 08/16/15 Pct Recovery = 81% Analysis Date = 08/11/15 Pct Recovery = 81% Analysis Date = 08/11/15 Pct Recovery = 81% Analysis Date = 08/06/15 Pct Recovery = 81% Analysis Date = 08/06/15 Pct Recovery = 81% Analysis Date = 08/01/15 Pct Recovery = 81% Analysis Date = 08/01/15 Pct Recovery = 81% Analysis Date = 07/27/15 Pct Recovery = 81% Analysis Date = 07/27/15 Pct Recovery = 81% Analysis Date = 07/22/15 Pct Recovery = 80% Analysis Date = 07/22/15 Pct Recovery = 80% Analysis Date = 07/17/15 Pct Recovery = 80% Analysis Date = 07/17/15 Pct Recovery = 80% Analysis Date = 07/12/15 Pct Recovery = 80% Analysis Date = 07/12/15 Pct Recovery = 80% Analysis Date = 07/07/15 Pct Recovery = 80% Analysis Date = 07/07/15 Pct Recovery = 80% Analysis Date = 07/02/15 Pct Recovery = 80% Analysis Date = 07/02/15 Pct Recovery = 80% Analysis Date = 06/27/15 Pct Recovery = 80% Analysis Date = 06/27/15 Pct Recovery = 80% Analysis Date = 06/22/15 Pct Recovery = 80% Analysis Date = 06/22/15 Pct Recovery = 80% Analysis Date = 06/17/15 Pct Recovery = 79% Analysis Date = 06/17/15 Pct Recovery = 79% Analysis Date = 06/12/15 Pct Recovery = 79% Analysis Date = 06/12/15 Pct Recovery = 79% Analysis Date = 06/07/15 Pct Recovery = 79% Analysis Date = 06/07/15 Pct Recovery = 79% Analysis Date = 06/02/15 Pct Recovery = 79% Analysis Date = 06/02/15 Pct Recovery = 79% Analysis Date = 05/28/15 Pct Recovery = 79% Analysis Date = 05/28/15 Pct Recovery = 79% Analysis Date = 05/23/15 Pct Recovery = 79% Analysis Date = 05/23/15 Pct Recovery = 79% Analysis Date = 05/18/15 Pct Recovery = 79% Analysis Date = 05/18/15 Pct Recovery = 79% Analysis Date = 05/13/15 Pct Recovery = 79% Analysis Date = 05/13/15 Pct Recovery = 79% Analysis Date = 05/08/15 Pct Recovery = 78% Analysis Date = 05/08/15 Pct Recovery = 78% Analysis Date = 05/03/15 Pct Recovery = 78% Analysis Date = 05/03/15 Pct Recovery = 78% Analysis Date = 04/28/15 Pct Recovery = 78% Analysis Date = 04/28/15 Pct Recovery = 78% Analysis Date = 04/23/15 Pct Recovery = 78% Analysis Date = 04/23/15 Pct Recovery = 78% Analysis Date = 04/18/15 Pct Recovery = 78% Analysis Date = 04/18/15 Pct Recovery = 78% Analysis Date = 04/13/15 Pct Recovery = 78% Analysis Date = 04/13/15 Pct Recovery = 78% Analysis Date = 04/08/15 Pct Recovery = 78% Analysis Date = 04/08/15 Pct Recovery = 78% Analysis Date = 04/03/15 Pct Recovery = 78% Analysis Date = 04/03/15 Pct Recovery = 78% Analysis Date = 03/29/15 Pct Recovery = 77% Analysis Date = 03/29/15 Pct Recovery = 77% Analysis Date = 03/24/15 Pct Recovery = 77% Analysis Date = 03/24/15 Pct Recovery = 77% Analysis Date = 03/19/15 Pct Recovery = 77% Analysis Date = 03/19/15 Pct Recovery = 77% Analysis Date = 03/14/15 Pct Recovery = 77% Analysis Date = 03/14/15 Pct Recovery = 77% Analysis Date = 03/09/15 Pct Recovery = 77% Analysis Date = 03/09/15 Pct Recovery = 77% Analysis Date = 03/04/15 Pct Recovery = 77% Analysis Date = 03/04/15 Pct Recovery = 77% Analysis Date = 02/27/15 Pct Recovery = 77% Analysis Date = 02/27/15 Pct Recovery = 77% Analysis Date = 02/22/15 Pct Recovery = 77% Analysis Date = 02/22/15 Pct Recovery = 77% Analysis Date = 02/17/15 Pct Recovery = 76% Analysis Date = 02/17/15 Pct Recovery = 76% Analysis Date = 02/12/15 Pct Recovery = 76% Analysis Date = 02/12/15 Pct Recovery = 76% Analysis Date = 02/07/15 Pct Recovery = 76% Analysis Date = 02/07/15 Pct Recovery = 76% Analysis Date = 02/02/15 Pct Recovery = 76% Analysis Date = 02/02/15 Pct Recovery = 76% Analysis Date = 01/28/15 Pct Recovery = 76% Analysis Date = 01/28/15 Pct Recovery = 76% Analysis Date = 01/23/15 Pct Recovery = 76% Analysis Date = 01/23/15 Pct Recovery = 76% Analysis Date = 01/18/15 Pct Recovery = 76% Analysis Date = 01/18/15 Pct Recovery = 76% Analysis Date = 01/13/15 Pct Recovery = 76% Analysis Date = 01/13/15 Pct Recovery = 76% Analysis Date = 01/08/15 Pct Recovery = 75% Analysis Date = 01/08/15 Pct Recovery = 75% Analysis Date = 01/03/15 Pct Recovery = 75% Analysis Date = 01/03/15 Pct Recovery = 75% Analysis Date = 12/29/14 Pct Recovery = 75% Analysis Date = 12/29/14 Pct Recovery = 75% Analysis Date = 12/24/14 Pct Recovery = 75% Analysis Date = 12/24/14 Pct Recovery = 75% Analysis Date = 12/19/14 Pct Recovery = 75% Analysis Date = 12/19/14 Pct Recovery = 75% Analysis Date = 12/14/14 Pct Recovery = 75% Analysis Date = 12/14/14 Pct Recovery = 75% Analysis Date = 12/09/14 Pct Recovery = 75% Analysis Date = 12/09/14 Pct Recovery = 75% Analysis Date = 12/04/14 Pct Recovery = 74% Analysis Date = 12/04/14 Pct Recovery = 74% Analysis Date = 11/29/14 Pct Recovery = 74% Analysis Date = 11/29/14 Pct Recovery = 74% Analysis Date = 11/24/14 Pct Recovery = 74% Analysis Date = 11/24/14 Pct Recovery = 74% Analysis Date = 11/19/14 Pct Recovery = 74% Analysis Date = 11/19/14 Pct Recovery = 74% Analysis Date = 11/14/14 Pct Recovery = 74% Analysis Date = 11/14/14 Pct Recovery = 74% Analysis Date = 11/09/14 Pct Recovery = 74% Analysis Date = 11/09/14 Pct Recovery = 74% Analysis Date = 11/04/14 Pct Recovery = 74% Analysis Date = 11/04/14 Pct Recovery = 74% Analysis Date = 10/30/14 Pct Recovery = 73% Analysis Date = 10/30/14 Pct Recovery = 73% Analysis Date = 10/25/14 Pct Recovery = 73% Analysis Date = 10/25/14 Pct Recovery = 73% Analysis Date = 10/20/14 Pct Recovery = 73% Analysis Date = 10/20/14 Pct Recovery = 73% Analysis Date = 10/15/14 Pct Recovery = 73% Analysis Date = 10/15/14 Pct Recovery = 73% Analysis Date = 10/10/14 Pct Recovery = 73% Analysis Date = 10/10/14 Pct Recovery = 73% Analysis Date = 10/05/14 Pct Recovery = 73% Analysis Date = 10/05/14 Pct Recovery = 73% Analysis Date = 09/30/14 Pct Recovery = 72% Analysis Date = 09/30/14 Pct Recovery = 72% Analysis Date = 09/25/14 Pct Recovery = 72% Analysis Date = 09/25/14 Pct Recovery = 72% Analysis Date = 09/20/14 Pct Recovery = 72% Analysis Date = 09/20/14 Pct Recovery = 72% Analysis Date = 09/15/14 Pct Recovery = 72% Analysis Date = 09/15/14 Pct Recovery = 72% Analysis Date = 09/10/14 Pct Recovery = 72% Analysis Date = 09/10/14 Pct Recovery = 72% Analysis Date = 09/05/14 Pct Recovery = 72% Analysis Date = 09/05/14 Pct Recovery = 72% Analysis Date = 08/31/14 Pct Recovery = 71% Analysis Date = 08/31/14 Pct Recovery = 71% Analysis Date = 08/26/14 Pct Recovery = 71% Analysis Date = 08/26/14 Pct Recovery = 71% Analysis Date = 08/21/14 Pct Recovery = 71% Analysis Date = 08/21/14 Pct Recovery = 71% Analysis Date = 08/16/14 Pct Recovery = 71% Analysis Date = 08/16/14 Pct Recovery = 71% Analysis Date = 08/11/14 Pct Recovery = 71% Analysis Date = 08/11/14 Pct Recovery = 71% Analysis Date = 08/06/14 Pct Recovery = 70% Analysis Date = 08/06/14 Pct Recovery = 70% Analysis Date = 08/01/14 Pct Recovery = 70% Analysis Date = 08/01/14 Pct Recovery = 70% Analysis Date = 07/27/14 Pct Recovery = 70% Analysis Date = 07/27/14 Pct Recovery = 70% Analysis Date = 07/22/14 Pct Recovery = 70% Analysis Date = 07/22/14 Pct Recovery = 70% Analysis Date = 07/17/14 Pct Recovery = 70% Analysis Date = 07/17/14 Pct Recovery = 70% Analysis Date = 07/12/14 Pct Recovery = 70% Analysis Date = 07/12/14 Pct Recovery = 70% Analysis Date = 07/07/14 Pct Recovery = 69% Analysis Date = 07/07/14 Pct Recovery = 69% Analysis Date = 07/02/14 Pct Recovery = 69% Analysis Date = 07/02/14 Pct Recovery = 69% Analysis Date = 06/27/14 Pct Recovery = 69% Analysis Date = 06/27/14 Pct Recovery = 69% Analysis Date = 06/22/14 Pct Recovery = 69% Analysis Date = 06/22/14 Pct Recovery = 69% Analysis Date = 06/17/14 Pct Recovery = 69% Analysis Date = 06/17/14 Pct Recovery = 69% Analysis Date = 06/12/14 Pct Recovery = 68% Analysis Date = 06/12/14 Pct Recovery = 68% Analysis Date = 06/07/14 Pct Recovery = 68% Analysis Date = 06/07/14 Pct Recovery = 68% Analysis Date = 06/02/14 Pct Recovery = 68% Analysis Date = 06/02/14 Pct Recovery = 68% Analysis Date = 05/28/14 Pct Recovery = 68% Analysis Date = 05/28/14 Pct Recovery = 68% Analysis Date = 05/23/14 Pct Recovery = 68% Analysis Date = 05/23/14 Pct Recovery = 68% Analysis Date = 05/18/14 Pct Recovery = 68% Analysis Date = 05/18/14 Pct Recovery = 68% Analysis Date = 05/13/14 Pct Recovery = 67% Analysis Date = 05/13/14 Pct Recovery = 67% Analysis Date = 05/08/14 Pct Recovery = 67% Analysis Date = 05/08/14 Pct Recovery = 67% Analysis Date = 05/03/14 Pct Recovery = 67% Analysis Date = 05/03/14 Pct Recovery = 67% Analysis Date = 04/28/14 Pct Recovery = 67% Analysis Date = 04/28/14 Pct Recovery = 67% Analysis Date = 04/23/14 Pct Recovery = 67% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
ALBUTEROL (SALBUTAMOL)

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 1 87% . 87% 0%
>= Reporting Level 74 76% 15% 77% 13%
Total 75 76% 15% 77% 14%

Sample Statistics
ALBUTEROL (SALBUTAMOL)

Characteristic N % % Basis
Plotted 75 99% Spiked
Estimated Values 9 12% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 1 1% Spiked
Spiked 76 .  
False Negatives 0 0% 0 out of 76
Not Spiked 39 .  
False Positives 0 0% 0 out of 39

BQS OBSP Determination:
ALPRAZOLAM
METHOD: 2440 , TESTIDCODE: 68250LCM56
Open Data Set

Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 96% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 90% Analysis Date = 11/24/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 82% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 80 µl & Abs 051315: 80 µl Pct Recovery = 51% Analysis Date = 11/18/16 SpikeMix = ERA 04281604: 80 µl & ERA 04281603: 80 µl Pct Recovery = 72% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & ERA 04281604: 80 µl Pct Recovery = 78% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 71% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 70% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 78% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 80% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 85% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 79% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-04: 15 µl & Abs 041814: 15 µl Pct Recovery = 93% Analysis Date = 02/06/15 SpikeMix = Abs 041814: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 89% Analysis Date = 07/12/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 85% Analysis Date = 06/22/14 SpikeMix = Abs 041814: 60 µl & Abs 041614: 60 µl Pct Recovery = 107% Analysis Date = 05/21/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 85% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 75% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 68% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-07A: 40 µl & Abs 051315: 40 µl Pct Recovery = 71% Analysis Date = 07/31/15 SpikeMix = Abs 051315: 40 µl & Abs 052215: 40 µl Pct Recovery = 59% Analysis Date = 07/30/15 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 77% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 71% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 69% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 68% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 76% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 101% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 118% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 85% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 87% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 85% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 91% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 59% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 62% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 74% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 82% Analysis Date = 04/10/15 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 90% Analysis Date = 11/04/14 SpikeMix = Abs 041814: 8 µl & ERA 0318-14-02: 8 µl Pct Recovery = 93% Analysis Date = 10/11/14 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 73% Analysis Date = 10/10/14 SpikeMix = Abs 041714: 30 µl & Abs 041814: 30 µl Pct Recovery = 75% Analysis Date = 10/10/14 SpikeMix = Abs 041814: 30 µl & ERA 0318-14-02: 30 µl Pct Recovery = 78% Analysis Date = 07/13/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 103% Analysis Date = 05/30/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 77% Analysis Date = 02/23/16 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 73% Analysis Date = 08/11/15 SpikeMix = Abs 050115: 20 µl & Abs 051315: 20 µl Pct Recovery = 53% Analysis Date = 06/26/15 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 76% Analysis Date = 06/09/15 SpikeMix = Abs 051315: 20 µl & Abs 050115: 20 µl Pct Recovery = 100% Analysis Date = 04/09/16 SpikeMix = Abs 051315: 10 µl & ERA 0406-15-09: 10 µl Pct Recovery = 37% Analysis Date = 04/09/16 SpikeMix = Abs 051315: 10 µl & ERA 0406-15-09: 10 µl Pct Recovery = 110% Analysis Date = 01/18/17 Pct Recovery = 92% Analysis Date = 01/14/17 Pct Recovery = 91% Analysis Date = 01/14/17 Pct Recovery = 91% Analysis Date = 01/09/17 Pct Recovery = 91% Analysis Date = 01/09/17 Pct Recovery = 91% Analysis Date = 01/04/17 Pct Recovery = 90% Analysis Date = 01/04/17 Pct Recovery = 90% Analysis Date = 12/30/16 Pct Recovery = 89% Analysis Date = 12/30/16 Pct Recovery = 89% Analysis Date = 12/25/16 Pct Recovery = 89% Analysis Date = 12/25/16 Pct Recovery = 89% Analysis Date = 12/20/16 Pct Recovery = 88% Analysis Date = 12/20/16 Pct Recovery = 88% Analysis Date = 12/15/16 Pct Recovery = 88% Analysis Date = 12/15/16 Pct Recovery = 88% Analysis Date = 12/11/16 Pct Recovery = 87% Analysis Date = 12/11/16 Pct Recovery = 87% Analysis Date = 12/06/16 Pct Recovery = 86% Analysis Date = 12/06/16 Pct Recovery = 86% Analysis Date = 12/01/16 Pct Recovery = 86% Analysis Date = 12/01/16 Pct Recovery = 86% Analysis Date = 11/26/16 Pct Recovery = 85% Analysis Date = 11/26/16 Pct Recovery = 85% Analysis Date = 11/21/16 Pct Recovery = 85% Analysis Date = 11/21/16 Pct Recovery = 85% Analysis Date = 11/16/16 Pct Recovery = 84% Analysis Date = 11/16/16 Pct Recovery = 84% Analysis Date = 11/11/16 Pct Recovery = 84% Analysis Date = 11/11/16 Pct Recovery = 84% Analysis Date = 11/06/16 Pct Recovery = 83% Analysis Date = 11/06/16 Pct Recovery = 83% Analysis Date = 11/02/16 Pct Recovery = 82% Analysis Date = 11/02/16 Pct Recovery = 82% Analysis Date = 10/28/16 Pct Recovery = 82% Analysis Date = 10/28/16 Pct Recovery = 82% Analysis Date = 10/23/16 Pct Recovery = 81% Analysis Date = 10/23/16 Pct Recovery = 81% Analysis Date = 10/18/16 Pct Recovery = 81% Analysis Date = 10/18/16 Pct Recovery = 81% Analysis Date = 10/13/16 Pct Recovery = 80% Analysis Date = 10/13/16 Pct Recovery = 80% Analysis Date = 10/08/16 Pct Recovery = 80% Analysis Date = 10/08/16 Pct Recovery = 80% Analysis Date = 10/03/16 Pct Recovery = 79% Analysis Date = 10/03/16 Pct Recovery = 79% Analysis Date = 09/28/16 Pct Recovery = 79% Analysis Date = 09/28/16 Pct Recovery = 79% Analysis Date = 09/24/16 Pct Recovery = 78% Analysis Date = 09/24/16 Pct Recovery = 78% Analysis Date = 09/19/16 Pct Recovery = 78% Analysis Date = 09/19/16 Pct Recovery = 78% Analysis Date = 09/14/16 Pct Recovery = 77% Analysis Date = 09/14/16 Pct Recovery = 77% Analysis Date = 09/09/16 Pct Recovery = 77% Analysis Date = 09/09/16 Pct Recovery = 77% Analysis Date = 09/04/16 Pct Recovery = 77% Analysis Date = 09/04/16 Pct Recovery = 77% Analysis Date = 08/30/16 Pct Recovery = 76% Analysis Date = 08/30/16 Pct Recovery = 76% Analysis Date = 08/25/16 Pct Recovery = 76% Analysis Date = 08/25/16 Pct Recovery = 76% Analysis Date = 08/21/16 Pct Recovery = 76% Analysis Date = 08/21/16 Pct Recovery = 76% Analysis Date = 08/16/16 Pct Recovery = 76% Analysis Date = 08/16/16 Pct Recovery = 76% Analysis Date = 08/11/16 Pct Recovery = 75% Analysis Date = 08/11/16 Pct Recovery = 75% Analysis Date = 08/06/16 Pct Recovery = 75% Analysis Date = 08/06/16 Pct Recovery = 75% Analysis Date = 08/01/16 Pct Recovery = 75% Analysis Date = 08/01/16 Pct Recovery = 75% Analysis Date = 07/27/16 Pct Recovery = 75% Analysis Date = 07/27/16 Pct Recovery = 75% Analysis Date = 07/22/16 Pct Recovery = 75% Analysis Date = 07/22/16 Pct Recovery = 75% Analysis Date = 07/17/16 Pct Recovery = 75% Analysis Date = 07/17/16 Pct Recovery = 75% Analysis Date = 07/13/16 Pct Recovery = 75% Analysis Date = 07/13/16 Pct Recovery = 75% Analysis Date = 07/08/16 Pct Recovery = 75% Analysis Date = 07/08/16 Pct Recovery = 75% Analysis Date = 07/03/16 Pct Recovery = 75% Analysis Date = 07/03/16 Pct Recovery = 75% Analysis Date = 06/28/16 Pct Recovery = 75% Analysis Date = 06/28/16 Pct Recovery = 75% Analysis Date = 06/23/16 Pct Recovery = 75% Analysis Date = 06/23/16 Pct Recovery = 75% Analysis Date = 06/18/16 Pct Recovery = 75% Analysis Date = 06/18/16 Pct Recovery = 75% Analysis Date = 06/13/16 Pct Recovery = 75% Analysis Date = 06/13/16 Pct Recovery = 75% Analysis Date = 06/08/16 Pct Recovery = 75% Analysis Date = 06/08/16 Pct Recovery = 75% Analysis Date = 06/04/16 Pct Recovery = 74% Analysis Date = 06/04/16 Pct Recovery = 74% Analysis Date = 05/30/16 Pct Recovery = 74% Analysis Date = 05/30/16 Pct Recovery = 74% Analysis Date = 05/25/16 Pct Recovery = 74% Analysis Date = 05/25/16 Pct Recovery = 74% Analysis Date = 05/20/16 Pct Recovery = 74% Analysis Date = 05/20/16 Pct Recovery = 74% Analysis Date = 05/15/16 Pct Recovery = 74% Analysis Date = 05/15/16 Pct Recovery = 74% Analysis Date = 05/10/16 Pct Recovery = 74% Analysis Date = 05/10/16 Pct Recovery = 74% Analysis Date = 05/05/16 Pct Recovery = 74% Analysis Date = 05/05/16 Pct Recovery = 74% Analysis Date = 05/01/16 Pct Recovery = 74% Analysis Date = 05/01/16 Pct Recovery = 74% Analysis Date = 04/26/16 Pct Recovery = 74% Analysis Date = 04/26/16 Pct Recovery = 74% Analysis Date = 04/21/16 Pct Recovery = 74% Analysis Date = 04/21/16 Pct Recovery = 74% Analysis Date = 04/16/16 Pct Recovery = 74% Analysis Date = 04/16/16 Pct Recovery = 74% Analysis Date = 04/11/16 Pct Recovery = 74% Analysis Date = 04/11/16 Pct Recovery = 74% Analysis Date = 04/06/16 Pct Recovery = 74% Analysis Date = 04/06/16 Pct Recovery = 74% Analysis Date = 04/01/16 Pct Recovery = 73% Analysis Date = 04/01/16 Pct Recovery = 73% Analysis Date = 03/27/16 Pct Recovery = 73% Analysis Date = 03/27/16 Pct Recovery = 73% Analysis Date = 03/23/16 Pct Recovery = 73% Analysis Date = 03/23/16 Pct Recovery = 73% Analysis Date = 03/18/16 Pct Recovery = 73% Analysis Date = 03/18/16 Pct Recovery = 73% Analysis Date = 03/13/16 Pct Recovery = 73% Analysis Date = 03/13/16 Pct Recovery = 73% Analysis Date = 03/08/16 Pct Recovery = 73% Analysis Date = 03/08/16 Pct Recovery = 73% Analysis Date = 03/03/16 Pct Recovery = 73% Analysis Date = 03/03/16 Pct Recovery = 73% Analysis Date = 02/27/16 Pct Recovery = 73% Analysis Date = 02/27/16 Pct Recovery = 73% Analysis Date = 02/22/16 Pct Recovery = 73% Analysis Date = 02/22/16 Pct Recovery = 73% Analysis Date = 02/17/16 Pct Recovery = 73% Analysis Date = 02/17/16 Pct Recovery = 73% Analysis Date = 02/13/16 Pct Recovery = 73% Analysis Date = 02/13/16 Pct Recovery = 73% Analysis Date = 02/08/16 Pct Recovery = 73% Analysis Date = 02/08/16 Pct Recovery = 73% Analysis Date = 02/03/16 Pct Recovery = 73% Analysis Date = 02/03/16 Pct Recovery = 73% Analysis Date = 01/29/16 Pct Recovery = 73% Analysis Date = 01/29/16 Pct Recovery = 73% Analysis Date = 01/24/16 Pct Recovery = 73% Analysis Date = 01/24/16 Pct Recovery = 73% Analysis Date = 01/19/16 Pct Recovery = 73% Analysis Date = 01/19/16 Pct Recovery = 73% Analysis Date = 01/14/16 Pct Recovery = 73% Analysis Date = 01/14/16 Pct Recovery = 73% Analysis Date = 01/10/16 Pct Recovery = 73% Analysis Date = 01/10/16 Pct Recovery = 73% Analysis Date = 01/05/16 Pct Recovery = 73% Analysis Date = 01/05/16 Pct Recovery = 73% Analysis Date = 12/31/15 Pct Recovery = 73% Analysis Date = 12/31/15 Pct Recovery = 73% Analysis Date = 12/26/15 Pct Recovery = 73% Analysis Date = 12/26/15 Pct Recovery = 73% Analysis Date = 12/21/15 Pct Recovery = 72% Analysis Date = 12/21/15 Pct Recovery = 72% Analysis Date = 12/16/15 Pct Recovery = 72% Analysis Date = 12/16/15 Pct Recovery = 72% Analysis Date = 12/11/15 Pct Recovery = 72% Analysis Date = 12/11/15 Pct Recovery = 72% Analysis Date = 12/06/15 Pct Recovery = 72% Analysis Date = 12/06/15 Pct Recovery = 72% Analysis Date = 12/02/15 Pct Recovery = 72% Analysis Date = 12/02/15 Pct Recovery = 72% Analysis Date = 11/27/15 Pct Recovery = 72% Analysis Date = 11/27/15 Pct Recovery = 72% Analysis Date = 11/22/15 Pct Recovery = 72% Analysis Date = 11/22/15 Pct Recovery = 72% Analysis Date = 11/17/15 Pct Recovery = 72% Analysis Date = 11/17/15 Pct Recovery = 72% Analysis Date = 11/12/15 Pct Recovery = 73% Analysis Date = 11/12/15 Pct Recovery = 73% Analysis Date = 11/07/15 Pct Recovery = 73% Analysis Date = 11/07/15 Pct Recovery = 73% Analysis Date = 11/02/15 Pct Recovery = 73% Analysis Date = 11/02/15 Pct Recovery = 73% Analysis Date = 10/28/15 Pct Recovery = 73% Analysis Date = 10/28/15 Pct Recovery = 73% Analysis Date = 10/24/15 Pct Recovery = 73% Analysis Date = 10/24/15 Pct Recovery = 73% Analysis Date = 10/19/15 Pct Recovery = 73% Analysis Date = 10/19/15 Pct Recovery = 73% Analysis Date = 10/14/15 Pct Recovery = 74% Analysis Date = 10/14/15 Pct Recovery = 74% Analysis Date = 10/09/15 Pct Recovery = 74% Analysis Date = 10/09/15 Pct Recovery = 74% Analysis Date = 10/04/15 Pct Recovery = 74% Analysis Date = 10/04/15 Pct Recovery = 74% Analysis Date = 09/29/15 Pct Recovery = 74% Analysis Date = 09/29/15 Pct Recovery = 74% Analysis Date = 09/24/15 Pct Recovery = 74% Analysis Date = 09/24/15 Pct Recovery = 74% Analysis Date = 09/19/15 Pct Recovery = 74% Analysis Date = 09/19/15 Pct Recovery = 74% Analysis Date = 09/15/15 Pct Recovery = 75% Analysis Date = 09/15/15 Pct Recovery = 75% Analysis Date = 09/10/15 Pct Recovery = 75% Analysis Date = 09/10/15 Pct Recovery = 75% Analysis Date = 09/05/15 Pct Recovery = 75% Analysis Date = 09/05/15 Pct Recovery = 75% Analysis Date = 08/31/15 Pct Recovery = 75% Analysis Date = 08/31/15 Pct Recovery = 75% Analysis Date = 08/26/15 Pct Recovery = 75% Analysis Date = 08/26/15 Pct Recovery = 75% Analysis Date = 08/21/15 Pct Recovery = 75% Analysis Date = 08/21/15 Pct Recovery = 75% Analysis Date = 08/16/15 Pct Recovery = 75% Analysis Date = 08/16/15 Pct Recovery = 75% Analysis Date = 08/12/15 Pct Recovery = 76% Analysis Date = 08/12/15 Pct Recovery = 76% Analysis Date = 08/07/15 Pct Recovery = 76% Analysis Date = 08/07/15 Pct Recovery = 76% Analysis Date = 08/02/15 Pct Recovery = 76% Analysis Date = 08/02/15 Pct Recovery = 76% Analysis Date = 07/28/15 Pct Recovery = 76% Analysis Date = 07/28/15 Pct Recovery = 76% Analysis Date = 07/23/15 Pct Recovery = 76% Analysis Date = 07/23/15 Pct Recovery = 76% Analysis Date = 07/18/15 Pct Recovery = 76% Analysis Date = 07/18/15 Pct Recovery = 76% Analysis Date = 07/13/15 Pct Recovery = 76% Analysis Date = 07/13/15 Pct Recovery = 76% Analysis Date = 07/08/15 Pct Recovery = 77% Analysis Date = 07/08/15 Pct Recovery = 77% Analysis Date = 07/04/15 Pct Recovery = 77% Analysis Date = 07/04/15 Pct Recovery = 77% Analysis Date = 06/29/15 Pct Recovery = 77% Analysis Date = 06/29/15 Pct Recovery = 77% Analysis Date = 06/24/15 Pct Recovery = 77% Analysis Date = 06/24/15 Pct Recovery = 77% Analysis Date = 06/19/15 Pct Recovery = 77% Analysis Date = 06/19/15 Pct Recovery = 77% Analysis Date = 06/14/15 Pct Recovery = 77% Analysis Date = 06/14/15 Pct Recovery = 77% Analysis Date = 06/09/15 Pct Recovery = 77% Analysis Date = 06/09/15 Pct Recovery = 77% Analysis Date = 06/04/15 Pct Recovery = 77% Analysis Date = 06/04/15 Pct Recovery = 77% Analysis Date = 05/30/15 Pct Recovery = 78% Analysis Date = 05/30/15 Pct Recovery = 78% Analysis Date = 05/26/15 Pct Recovery = 78% Analysis Date = 05/26/15 Pct Recovery = 78% Analysis Date = 05/21/15 Pct Recovery = 78% Analysis Date = 05/21/15 Pct Recovery = 78% Analysis Date = 05/16/15 Pct Recovery = 78% Analysis Date = 05/16/15 Pct Recovery = 78% Analysis Date = 05/11/15 Pct Recovery = 78% Analysis Date = 05/11/15 Pct Recovery = 78% Analysis Date = 05/06/15 Pct Recovery = 78% Analysis Date = 05/06/15 Pct Recovery = 78% Analysis Date = 05/01/15 Pct Recovery = 79% Analysis Date = 05/01/15 Pct Recovery = 79% Analysis Date = 04/26/15 Pct Recovery = 79% Analysis Date = 04/26/15 Pct Recovery = 79% Analysis Date = 04/22/15 Pct Recovery = 79% Analysis Date = 04/22/15 Pct Recovery = 79% Analysis Date = 04/17/15 Pct Recovery = 79% Analysis Date = 04/17/15 Pct Recovery = 79% Analysis Date = 04/12/15 Pct Recovery = 79% Analysis Date = 04/12/15 Pct Recovery = 79% Analysis Date = 04/07/15 Pct Recovery = 79% Analysis Date = 04/07/15 Pct Recovery = 79% Analysis Date = 04/02/15 Pct Recovery = 80% Analysis Date = 04/02/15 Pct Recovery = 80% Analysis Date = 03/28/15 Pct Recovery = 80% Analysis Date = 03/28/15 Pct Recovery = 80% Analysis Date = 03/23/15 Pct Recovery = 80% Analysis Date = 03/23/15 Pct Recovery = 80% Analysis Date = 03/18/15 Pct Recovery = 80% Analysis Date = 03/18/15 Pct Recovery = 80% Analysis Date = 03/14/15 Pct Recovery = 80% Analysis Date = 03/14/15 Pct Recovery = 80% Analysis Date = 03/09/15 Pct Recovery = 80% Analysis Date = 03/09/15 Pct Recovery = 80% Analysis Date = 03/04/15 Pct Recovery = 81% Analysis Date = 03/04/15 Pct Recovery = 81% Analysis Date = 02/27/15 Pct Recovery = 81% Analysis Date = 02/27/15 Pct Recovery = 81% Analysis Date = 02/22/15 Pct Recovery = 81% Analysis Date = 02/22/15 Pct Recovery = 81% Analysis Date = 02/17/15 Pct Recovery = 81% Analysis Date = 02/17/15 Pct Recovery = 81% Analysis Date = 02/12/15 Pct Recovery = 81% Analysis Date = 02/12/15 Pct Recovery = 81% Analysis Date = 02/07/15 Pct Recovery = 81% Analysis Date = 02/07/15 Pct Recovery = 81% Analysis Date = 02/03/15 Pct Recovery = 82% Analysis Date = 02/03/15 Pct Recovery = 82% Analysis Date = 01/29/15 Pct Recovery = 82% Analysis Date = 01/29/15 Pct Recovery = 82% Analysis Date = 01/24/15 Pct Recovery = 82% Analysis Date = 01/24/15 Pct Recovery = 82% Analysis Date = 01/19/15 Pct Recovery = 82% Analysis Date = 01/19/15 Pct Recovery = 82% Analysis Date = 01/14/15 Pct Recovery = 82% Analysis Date = 01/14/15 Pct Recovery = 82% Analysis Date = 01/09/15 Pct Recovery = 82% Analysis Date = 01/09/15 Pct Recovery = 82% Analysis Date = 01/04/15 Pct Recovery = 83% Analysis Date = 01/04/15 Pct Recovery = 83% Analysis Date = 12/31/14 Pct Recovery = 83% Analysis Date = 12/31/14 Pct Recovery = 83% Analysis Date = 12/26/14 Pct Recovery = 83% Analysis Date = 12/26/14 Pct Recovery = 83% Analysis Date = 12/21/14 Pct Recovery = 83% Analysis Date = 12/21/14 Pct Recovery = 83% Analysis Date = 12/16/14 Pct Recovery = 83% Analysis Date = 12/16/14 Pct Recovery = 83% Analysis Date = 12/11/14 Pct Recovery = 84% Analysis Date = 12/11/14 Pct Recovery = 84% Analysis Date = 12/06/14 Pct Recovery = 84% Analysis Date = 12/06/14 Pct Recovery = 84% Analysis Date = 12/01/14 Pct Recovery = 84% Analysis Date = 12/01/14 Pct Recovery = 84% Analysis Date = 11/26/14 Pct Recovery = 84% Analysis Date = 11/26/14 Pct Recovery = 84% Analysis Date = 11/22/14 Pct Recovery = 84% Analysis Date = 11/22/14 Pct Recovery = 84% Analysis Date = 11/17/14 Pct Recovery = 84% Analysis Date = 11/17/14 Pct Recovery = 84% Analysis Date = 11/12/14 Pct Recovery = 85% Analysis Date = 11/12/14 Pct Recovery = 85% Analysis Date = 11/07/14 Pct Recovery = 85% Analysis Date = 11/07/14 Pct Recovery = 85% Analysis Date = 11/02/14 Pct Recovery = 85% Analysis Date = 11/02/14 Pct Recovery = 85% Analysis Date = 10/28/14 Pct Recovery = 85% Analysis Date = 10/28/14 Pct Recovery = 85% Analysis Date = 10/23/14 Pct Recovery = 85% Analysis Date = 10/23/14 Pct Recovery = 85% Analysis Date = 10/18/14 Pct Recovery = 85% Analysis Date = 10/18/14 Pct Recovery = 85% Analysis Date = 10/14/14 Pct Recovery = 86% Analysis Date = 10/14/14 Pct Recovery = 86% Analysis Date = 10/09/14 Pct Recovery = 86% Analysis Date = 10/09/14 Pct Recovery = 86% Analysis Date = 10/04/14 Pct Recovery = 86% Analysis Date = 10/04/14 Pct Recovery = 86% Analysis Date = 09/29/14 Pct Recovery = 86% Analysis Date = 09/29/14 Pct Recovery = 86% Analysis Date = 09/24/14 Pct Recovery = 86% Analysis Date = 09/24/14 Pct Recovery = 86% Analysis Date = 09/19/14 Pct Recovery = 87% Analysis Date = 09/19/14 Pct Recovery = 87% Analysis Date = 09/14/14 Pct Recovery = 87% Analysis Date = 09/14/14 Pct Recovery = 87% Analysis Date = 09/10/14 Pct Recovery = 87% Analysis Date = 09/10/14 Pct Recovery = 87% Analysis Date = 09/05/14 Pct Recovery = 87% Analysis Date = 09/05/14 Pct Recovery = 87% Analysis Date = 08/31/14 Pct Recovery = 87% Analysis Date = 08/31/14 Pct Recovery = 87% Analysis Date = 08/26/14 Pct Recovery = 87% Analysis Date = 08/26/14 Pct Recovery = 87% Analysis Date = 08/21/14 Pct Recovery = 88% Analysis Date = 08/21/14 Pct Recovery = 88% Analysis Date = 08/16/14 Pct Recovery = 88% Analysis Date = 08/16/14 Pct Recovery = 88% Analysis Date = 08/11/14 Pct Recovery = 88% Analysis Date = 08/11/14 Pct Recovery = 88% Analysis Date = 08/06/14 Pct Recovery = 88% Analysis Date = 08/06/14 Pct Recovery = 88% Analysis Date = 08/02/14 Pct Recovery = 88% Analysis Date = 08/02/14 Pct Recovery = 88% Analysis Date = 07/28/14 Pct Recovery = 88% Analysis Date = 07/28/14 Pct Recovery = 88% Analysis Date = 07/23/14 Pct Recovery = 89% Analysis Date = 07/23/14 Pct Recovery = 89% Analysis Date = 07/18/14 Pct Recovery = 89% Analysis Date = 07/18/14 Pct Recovery = 89% Analysis Date = 07/13/14 Pct Recovery = 89% Analysis Date = 07/13/14 Pct Recovery = 89% Analysis Date = 07/08/14 Pct Recovery = 89% Analysis Date = 07/08/14 Pct Recovery = 89% Analysis Date = 07/03/14 Pct Recovery = 89% Analysis Date = 07/03/14 Pct Recovery = 89% Analysis Date = 06/28/14 Pct Recovery = 89% Analysis Date = 06/28/14 Pct Recovery = 89% Analysis Date = 06/24/14 Pct Recovery = 90% Analysis Date = 06/24/14 Pct Recovery = 90% Analysis Date = 06/19/14 Pct Recovery = 90% Analysis Date = 06/19/14 Pct Recovery = 90% Analysis Date = 06/14/14 Pct Recovery = 90% Analysis Date = 06/14/14 Pct Recovery = 90% Analysis Date = 06/09/14 Pct Recovery = 90% Analysis Date = 06/09/14 Pct Recovery = 90% Analysis Date = 06/04/14 Pct Recovery = 90% Analysis Date = 06/04/14 Pct Recovery = 90% Analysis Date = 05/30/14 Pct Recovery = 90% Analysis Date = 05/30/14 Pct Recovery = 90% Analysis Date = 05/25/14 Pct Recovery = 91% Analysis Date = 05/25/14 Pct Recovery = 91% Analysis Date = 05/21/14 Pct Recovery = 91% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
ALPRAZOLAM

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 2 74% 51% 74% 54%
>= Reporting Level 47 80% 14% 78% 13%
Total 49 80% 15% 78% 13%

Sample Statistics
ALPRAZOLAM

Characteristic N % % Basis
Plotted 49 98% Spiked
Estimated Values 12 24% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 50 .  
False Negatives 1 2% 1 out of 50
Not Spiked 65 .  
False Positives 12 18% 12 out of 65

BQS OBSP Determination:
AMITRIPTYLINE
METHOD: 2440 , TESTIDCODE: 67522LCM56
Open Data Set

Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 65% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 59% Analysis Date = 01/17/16 SpikeMix = ERA 0406-15-09: 80 µl & ERA 0406-15-07A: 80 µl Pct Recovery = 60% Analysis Date = 11/24/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 65% Analysis Date = 10/01/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 39% Analysis Date = 11/05/15 SpikeMix = ERA 0406-15-08: 80 µl & Abs 052215: 80 µl Pct Recovery = 63% Analysis Date = 11/04/15 SpikeMix = Abs 052215: 80 µl & Abs 050115: 80 µl Pct Recovery = 52% Analysis Date = 11/18/16 SpikeMix = ERA 04281604: 80 µl & ERA 04281603: 80 µl Pct Recovery = 60% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & ERA 04281604: 80 µl Pct Recovery = 50% Analysis Date = 09/24/16 SpikeMix = Crescent EN160610015: 80 µl & Abs 061416: 80 µl Pct Recovery = 60% Analysis Date = 09/24/16 SpikeMix = Abs 061416: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 65% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 79% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 78% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 72% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 75% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-04: 15 µl & Abs 041814: 15 µl Pct Recovery = 51% Analysis Date = 02/06/15 SpikeMix = Abs 041814: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 51% Analysis Date = 07/12/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 63% Analysis Date = 06/22/14 SpikeMix = Abs 041814: 60 µl & Abs 041614: 60 µl Pct Recovery = 73% Analysis Date = 05/21/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 59% Analysis Date = 05/07/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 55% Analysis Date = 04/29/15 SpikeMix = ERA 0319-14-05: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 62% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 56% Analysis Date = 01/16/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 55% Analysis Date = 12/07/14 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 59% Analysis Date = 12/06/14 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 45% Analysis Date = 08/28/14 SpikeMix = ERA 0319-14-04: 60 µl & ERA 0319-14-05: 60 µl Pct Recovery = 51% Analysis Date = 07/26/14 SpikeMix = ERA 0319-14-05: 60 µl & ERA 0318-14-02: 60 µl Pct Recovery = 67% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-08: 40 µl & ERA 0406-15-09: 40 µl Pct Recovery = 44% Analysis Date = 07/31/15 SpikeMix = ERA 0406-15-09: 40 µl & Abs 050115: 40 µl Pct Recovery = 62% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-08: 40 µl & Abs 052215: 40 µl Pct Recovery = 65% Analysis Date = 02/23/16 SpikeMix = Abs 052215: 40 µl & Abs 050115: 40 µl Pct Recovery = 67% Analysis Date = 09/10/15 SpikeMix = Abs 052215: 40 µl & ERA 0406-15-07A: 40 µl Pct Recovery = 65% Analysis Date = 07/31/15 SpikeMix = Abs 051315: 40 µl & Abs 052215: 40 µl Pct Recovery = 63% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 76% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 94% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 67% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 70% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 44% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 49% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 63% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 60% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 46% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 57% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 41% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 44% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 30% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 42% Analysis Date = 04/10/15 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 46% Analysis Date = 11/04/14 SpikeMix = Abs 041814: 8 µl & ERA 0318-14-02: 8 µl Pct Recovery = 32% Analysis Date = 10/11/14 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 43% Analysis Date = 11/04/14 SpikeMix = Abs 041714: 8 µl & ERA 0319-14-05: 8 µl Pct Recovery = 35% Analysis Date = 10/24/14 SpikeMix = ERA 0319-14-05: 8 µl & Abs 041614: 8 µl Pct Recovery = 44% Analysis Date = 10/10/14 SpikeMix = Abs 041714: 30 µl & Abs 041814: 30 µl Pct Recovery = 51% Analysis Date = 10/10/14 SpikeMix = Abs 041814: 30 µl & ERA 0318-14-02: 30 µl Pct Recovery = 52% Analysis Date = 07/13/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 60% Analysis Date = 05/30/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 54% Analysis Date = 08/30/14 SpikeMix = ERA 0318-14-02: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 56% Analysis Date = 08/16/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 27% Analysis Date = 07/13/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 31% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 34% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 43% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-08: 20 µl & ERA 0406-15-09: 20 µl Pct Recovery = 41% Analysis Date = 11/24/15 SpikeMix = ERA 0406-15-09: 20 µl & Abs 050115: 20 µl Pct Recovery = 58% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-09: 20 µl Pct Recovery = 12% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 51% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 55% Analysis Date = 02/23/16 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 57% Analysis Date = 11/24/15 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 54% Analysis Date = 09/09/15 SpikeMix = ERA 0406-15-08: 20 µl & Abs 052215: 20 µl Pct Recovery = 53% Analysis Date = 08/27/15 SpikeMix = Abs 052215: 20 µl & Abs 050115: 20 µl Pct Recovery = 65% Analysis Date = 07/09/15 SpikeMix = Abs 050115: 20 µl & Abs 052215: 20 µl Pct Recovery = 50% Analysis Date = 06/26/15 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 65% Analysis Date = 04/09/16 SpikeMix = Abs 051315: 10 µl & ERA 0406-15-09: 10 µl Pct Recovery = 12% Analysis Date = 04/09/16 SpikeMix = Abs 051315: 10 µl & ERA 0406-15-09: 10 µl Pct Recovery = 42% Analysis Date = 01/04/17 Pct Recovery = 66% Analysis Date = 12/31/16 Pct Recovery = 66% Analysis Date = 12/31/16 Pct Recovery = 66% Analysis Date = 12/26/16 Pct Recovery = 65% Analysis Date = 12/26/16 Pct Recovery = 65% Analysis Date = 12/21/16 Pct Recovery = 65% Analysis Date = 12/21/16 Pct Recovery = 65% Analysis Date = 12/16/16 Pct Recovery = 65% Analysis Date = 12/16/16 Pct Recovery = 65% Analysis Date = 12/11/16 Pct Recovery = 65% Analysis Date = 12/11/16 Pct Recovery = 65% Analysis Date = 12/07/16 Pct Recovery = 64% Analysis Date = 12/07/16 Pct Recovery = 64% Analysis Date = 12/02/16 Pct Recovery = 64% Analysis Date = 12/02/16 Pct Recovery = 64% Analysis Date = 11/27/16 Pct Recovery = 64% Analysis Date = 11/27/16 Pct Recovery = 64% Analysis Date = 11/22/16 Pct Recovery = 63% Analysis Date = 11/22/16 Pct Recovery = 63% Analysis Date = 11/17/16 Pct Recovery = 63% Analysis Date = 11/17/16 Pct Recovery = 63% Analysis Date = 11/13/16 Pct Recovery = 63% Analysis Date = 11/13/16 Pct Recovery = 63% Analysis Date = 11/08/16 Pct Recovery = 62% Analysis Date = 11/08/16 Pct Recovery = 62% Analysis Date = 11/03/16 Pct Recovery = 62% Analysis Date = 11/03/16 Pct Recovery = 62% Analysis Date = 10/29/16 Pct Recovery = 62% Analysis Date = 10/29/16 Pct Recovery = 62% Analysis Date = 10/24/16 Pct Recovery = 61% Analysis Date = 10/24/16 Pct Recovery = 61% Analysis Date = 10/20/16 Pct Recovery = 61% Analysis Date = 10/20/16 Pct Recovery = 61% Analysis Date = 10/15/16 Pct Recovery = 61% Analysis Date = 10/15/16 Pct Recovery = 61% Analysis Date = 10/10/16 Pct Recovery = 60% Analysis Date = 10/10/16 Pct Recovery = 60% Analysis Date = 10/05/16 Pct Recovery = 60% Analysis Date = 10/05/16 Pct Recovery = 60% Analysis Date = 09/30/16 Pct Recovery = 60% Analysis Date = 09/30/16 Pct Recovery = 60% Analysis Date = 09/26/16 Pct Recovery = 60% Analysis Date = 09/26/16 Pct Recovery = 60% Analysis Date = 09/21/16 Pct Recovery = 59% Analysis Date = 09/21/16 Pct Recovery = 59% Analysis Date = 09/16/16 Pct Recovery = 59% Analysis Date = 09/16/16 Pct Recovery = 59% Analysis Date = 09/11/16 Pct Recovery = 59% Analysis Date = 09/11/16 Pct Recovery = 59% Analysis Date = 09/06/16 Pct Recovery = 58% Analysis Date = 09/06/16 Pct Recovery = 58% Analysis Date = 09/02/16 Pct Recovery = 58% Analysis Date = 09/02/16 Pct Recovery = 58% Analysis Date = 08/28/16 Pct Recovery = 58% Analysis Date = 08/28/16 Pct Recovery = 58% Analysis Date = 08/23/16 Pct Recovery = 58% Analysis Date = 08/23/16 Pct Recovery = 58% Analysis Date = 08/18/16 Pct Recovery = 57% Analysis Date = 08/18/16 Pct Recovery = 57% Analysis Date = 08/13/16 Pct Recovery = 57% Analysis Date = 08/13/16 Pct Recovery = 57% Analysis Date = 08/09/16 Pct Recovery = 57% Analysis Date = 08/09/16 Pct Recovery = 57% Analysis Date = 08/04/16 Pct Recovery = 57% Analysis Date = 08/04/16 Pct Recovery = 57% Analysis Date = 07/30/16 Pct Recovery = 56% Analysis Date = 07/30/16 Pct Recovery = 56% Analysis Date = 07/25/16 Pct Recovery = 56% Analysis Date = 07/25/16 Pct Recovery = 56% Analysis Date = 07/20/16 Pct Recovery = 56% Analysis Date = 07/20/16 Pct Recovery = 56% Analysis Date = 07/16/16 Pct Recovery = 56% Analysis Date = 07/16/16 Pct Recovery = 56% Analysis Date = 07/11/16 Pct Recovery = 56% Analysis Date = 07/11/16 Pct Recovery = 56% Analysis Date = 07/06/16 Pct Recovery = 56% Analysis Date = 07/06/16 Pct Recovery = 56% Analysis Date = 07/01/16 Pct Recovery = 55% Analysis Date = 07/01/16 Pct Recovery = 55% Analysis Date = 06/26/16 Pct Recovery = 55% Analysis Date = 06/26/16 Pct Recovery = 55% Analysis Date = 06/22/16 Pct Recovery = 55% Analysis Date = 06/22/16 Pct Recovery = 55% Analysis Date = 06/17/16 Pct Recovery = 55% Analysis Date = 06/17/16 Pct Recovery = 55% Analysis Date = 06/12/16 Pct Recovery = 55% Analysis Date = 06/12/16 Pct Recovery = 55% Analysis Date = 06/07/16 Pct Recovery = 55% Analysis Date = 06/07/16 Pct Recovery = 55% Analysis Date = 06/02/16 Pct Recovery = 54% Analysis Date = 06/02/16 Pct Recovery = 54% Analysis Date = 05/29/16 Pct Recovery = 54% Analysis Date = 05/29/16 Pct Recovery = 54% Analysis Date = 05/24/16 Pct Recovery = 54% Analysis Date = 05/24/16 Pct Recovery = 54% Analysis Date = 05/19/16 Pct Recovery = 54% Analysis Date = 05/19/16 Pct Recovery = 54% Analysis Date = 05/14/16 Pct Recovery = 54% Analysis Date = 05/14/16 Pct Recovery = 54% Analysis Date = 05/09/16 Pct Recovery = 54% Analysis Date = 05/09/16 Pct Recovery = 54% Analysis Date = 05/05/16 Pct Recovery = 53% Analysis Date = 05/05/16 Pct Recovery = 53% Analysis Date = 04/30/16 Pct Recovery = 53% Analysis Date = 04/30/16 Pct Recovery = 53% Analysis Date = 04/25/16 Pct Recovery = 53% Analysis Date = 04/25/16 Pct Recovery = 53% Analysis Date = 04/20/16 Pct Recovery = 53% Analysis Date = 04/20/16 Pct Recovery = 53% Analysis Date = 04/15/16 Pct Recovery = 53% Analysis Date = 04/15/16 Pct Recovery = 53% Analysis Date = 04/11/16 Pct Recovery = 53% Analysis Date = 04/11/16 Pct Recovery = 53% Analysis Date = 04/06/16 Pct Recovery = 52% Analysis Date = 04/06/16 Pct Recovery = 52% Analysis Date = 04/01/16 Pct Recovery = 52% Analysis Date = 04/01/16 Pct Recovery = 52% Analysis Date = 03/27/16 Pct Recovery = 52% Analysis Date = 03/27/16 Pct Recovery = 52% Analysis Date = 03/22/16 Pct Recovery = 52% Analysis Date = 03/22/16 Pct Recovery = 52% Analysis Date = 03/18/16 Pct Recovery = 52% Analysis Date = 03/18/16 Pct Recovery = 52% Analysis Date = 03/13/16 Pct Recovery = 52% Analysis Date = 03/13/16 Pct Recovery = 52% Analysis Date = 03/08/16 Pct Recovery = 52% Analysis Date = 03/08/16 Pct Recovery = 52% Analysis Date = 03/03/16 Pct Recovery = 52% Analysis Date = 03/03/16 Pct Recovery = 52% Analysis Date = 02/27/16 Pct Recovery = 52% Analysis Date = 02/27/16 Pct Recovery = 52% Analysis Date = 02/23/16 Pct Recovery = 52% Analysis Date = 02/23/16 Pct Recovery = 52% Analysis Date = 02/18/16 Pct Recovery = 52% Analysis Date = 02/18/16 Pct Recovery = 52% Analysis Date = 02/13/16 Pct Recovery = 52% Analysis Date = 02/13/16 Pct Recovery = 52% Analysis Date = 02/08/16 Pct Recovery = 52% Analysis Date = 02/08/16 Pct Recovery = 52% Analysis Date = 02/03/16 Pct Recovery = 52% Analysis Date = 02/03/16 Pct Recovery = 52% Analysis Date = 01/30/16 Pct Recovery = 52% Analysis Date = 01/30/16 Pct Recovery = 52% Analysis Date = 01/25/16 Pct Recovery = 52% Analysis Date = 01/25/16 Pct Recovery = 52% Analysis Date = 01/20/16 Pct Recovery = 52% Analysis Date = 01/20/16 Pct Recovery = 52% Analysis Date = 01/15/16 Pct Recovery = 52% Analysis Date = 01/15/16 Pct Recovery = 52% Analysis Date = 01/10/16 Pct Recovery = 52% Analysis Date = 01/10/16 Pct Recovery = 52% Analysis Date = 01/06/16 Pct Recovery = 52% Analysis Date = 01/06/16 Pct Recovery = 52% Analysis Date = 01/01/16 Pct Recovery = 52% Analysis Date = 01/01/16 Pct Recovery = 52% Analysis Date = 12/27/15 Pct Recovery = 52% Analysis Date = 12/27/15 Pct Recovery = 52% Analysis Date = 12/22/15 Pct Recovery = 52% Analysis Date = 12/22/15 Pct Recovery = 52% Analysis Date = 12/17/15 Pct Recovery = 52% Analysis Date = 12/17/15 Pct Recovery = 52% Analysis Date = 12/13/15 Pct Recovery = 52% Analysis Date = 12/13/15 Pct Recovery = 52% Analysis Date = 12/08/15 Pct Recovery = 52% Analysis Date = 12/08/15 Pct Recovery = 52% Analysis Date = 12/03/15 Pct Recovery = 52% Analysis Date = 12/03/15 Pct Recovery = 52% Analysis Date = 11/28/15 Pct Recovery = 52% Analysis Date = 11/28/15 Pct Recovery = 52% Analysis Date = 11/23/15 Pct Recovery = 52% Analysis Date = 11/23/15 Pct Recovery = 52% Analysis Date = 11/19/15 Pct Recovery = 52% Analysis Date = 11/19/15 Pct Recovery = 52% Analysis Date = 11/14/15 Pct Recovery = 52% Analysis Date = 11/14/15 Pct Recovery = 52% Analysis Date = 11/09/15 Pct Recovery = 52% Analysis Date = 11/09/15 Pct Recovery = 52% Analysis Date = 11/04/15 Pct Recovery = 52% Analysis Date = 11/04/15 Pct Recovery = 52% Analysis Date = 10/30/15 Pct Recovery = 52% Analysis Date = 10/30/15 Pct Recovery = 52% Analysis Date = 10/26/15 Pct Recovery = 53% Analysis Date = 10/26/15 Pct Recovery = 53% Analysis Date = 10/21/15 Pct Recovery = 53% Analysis Date = 10/21/15 Pct Recovery = 53% Analysis Date = 10/16/15 Pct Recovery = 53% Analysis Date = 10/16/15 Pct Recovery = 53% Analysis Date = 10/11/15 Pct Recovery = 53% Analysis Date = 10/11/15 Pct Recovery = 53% Analysis Date = 10/06/15 Pct Recovery = 53% Analysis Date = 10/06/15 Pct Recovery = 53% Analysis Date = 10/02/15 Pct Recovery = 53% Analysis Date = 10/02/15 Pct Recovery = 53% Analysis Date = 09/27/15 Pct Recovery = 53% Analysis Date = 09/27/15 Pct Recovery = 53% Analysis Date = 09/22/15 Pct Recovery = 53% Analysis Date = 09/22/15 Pct Recovery = 53% Analysis Date = 09/17/15 Pct Recovery = 53% Analysis Date = 09/17/15 Pct Recovery = 53% Analysis Date = 09/12/15 Pct Recovery = 53% Analysis Date = 09/12/15 Pct Recovery = 53% Analysis Date = 09/08/15 Pct Recovery = 53% Analysis Date = 09/08/15 Pct Recovery = 53% Analysis Date = 09/03/15 Pct Recovery = 53% Analysis Date = 09/03/15 Pct Recovery = 53% Analysis Date = 08/29/15 Pct Recovery = 53% Analysis Date = 08/29/15 Pct Recovery = 53% Analysis Date = 08/24/15 Pct Recovery = 53% Analysis Date = 08/24/15 Pct Recovery = 53% Analysis Date = 08/19/15 Pct Recovery = 53% Analysis Date = 08/19/15 Pct Recovery = 53% Analysis Date = 08/15/15 Pct Recovery = 53% Analysis Date = 08/15/15 Pct Recovery = 53% Analysis Date = 08/10/15 Pct Recovery = 53% Analysis Date = 08/10/15 Pct Recovery = 53% Analysis Date = 08/05/15 Pct Recovery = 53% Analysis Date = 08/05/15 Pct Recovery = 53% Analysis Date = 07/31/15 Pct Recovery = 53% Analysis Date = 07/31/15 Pct Recovery = 53% Analysis Date = 07/26/15 Pct Recovery = 53% Analysis Date = 07/26/15 Pct Recovery = 53% Analysis Date = 07/22/15 Pct Recovery = 53% Analysis Date = 07/22/15 Pct Recovery = 53% Analysis Date = 07/17/15 Pct Recovery = 53% Analysis Date = 07/17/15 Pct Recovery = 53% Analysis Date = 07/12/15 Pct Recovery = 53% Analysis Date = 07/12/15 Pct Recovery = 53% Analysis Date = 07/07/15 Pct Recovery = 53% Analysis Date = 07/07/15 Pct Recovery = 53% Analysis Date = 07/02/15 Pct Recovery = 53% Analysis Date = 07/02/15 Pct Recovery = 53% Analysis Date = 06/28/15 Pct Recovery = 53% Analysis Date = 06/28/15 Pct Recovery = 53% Analysis Date = 06/23/15 Pct Recovery = 53% Analysis Date = 06/23/15 Pct Recovery = 53% Analysis Date = 06/18/15 Pct Recovery = 52% Analysis Date = 06/18/15 Pct Recovery = 52% Analysis Date = 06/13/15 Pct Recovery = 52% Analysis Date = 06/13/15 Pct Recovery = 52% Analysis Date = 06/08/15 Pct Recovery = 52% Analysis Date = 06/08/15 Pct Recovery = 52% Analysis Date = 06/04/15 Pct Recovery = 52% Analysis Date = 06/04/15 Pct Recovery = 52% Analysis Date = 05/30/15 Pct Recovery = 52% Analysis Date = 05/30/15 Pct Recovery = 52% Analysis Date = 05/25/15 Pct Recovery = 52% Analysis Date = 05/25/15 Pct Recovery = 52% Analysis Date = 05/20/15 Pct Recovery = 52% Analysis Date = 05/20/15 Pct Recovery = 52% Analysis Date = 05/15/15 Pct Recovery = 52% Analysis Date = 05/15/15 Pct Recovery = 52% Analysis Date = 05/11/15 Pct Recovery = 52% Analysis Date = 05/11/15 Pct Recovery = 52% Analysis Date = 05/06/15 Pct Recovery = 52% Analysis Date = 05/06/15 Pct Recovery = 52% Analysis Date = 05/01/15 Pct Recovery = 52% Analysis Date = 05/01/15 Pct Recovery = 52% Analysis Date = 04/26/15 Pct Recovery = 52% Analysis Date = 04/26/15 Pct Recovery = 52% Analysis Date = 04/21/15 Pct Recovery = 52% Analysis Date = 04/21/15 Pct Recovery = 52% Analysis Date = 04/17/15 Pct Recovery = 52% Analysis Date = 04/17/15 Pct Recovery = 52% Analysis Date = 04/12/15 Pct Recovery = 52% Analysis Date = 04/12/15 Pct Recovery = 52% Analysis Date = 04/07/15 Pct Recovery = 52% Analysis Date = 04/07/15 Pct Recovery = 52% Analysis Date = 04/02/15 Pct Recovery = 52% Analysis Date = 04/02/15 Pct Recovery = 52% Analysis Date = 03/28/15 Pct Recovery = 52% Analysis Date = 03/28/15 Pct Recovery = 52% Analysis Date = 03/24/15 Pct Recovery = 52% Analysis Date = 03/24/15 Pct Recovery = 52% Analysis Date = 03/19/15 Pct Recovery = 52% Analysis Date = 03/19/15 Pct Recovery = 52% Analysis Date = 03/14/15 Pct Recovery = 52% Analysis Date = 03/14/15 Pct Recovery = 52% Analysis Date = 03/09/15 Pct Recovery = 52% Analysis Date = 03/09/15 Pct Recovery = 52% Analysis Date = 03/04/15 Pct Recovery = 52% Analysis Date = 03/04/15 Pct Recovery = 52% Analysis Date = 02/28/15 Pct Recovery = 52% Analysis Date = 02/28/15 Pct Recovery = 52% Analysis Date = 02/23/15 Pct Recovery = 52% Analysis Date = 02/23/15 Pct Recovery = 52% Analysis Date = 02/18/15 Pct Recovery = 52% Analysis Date = 02/18/15 Pct Recovery = 52% Analysis Date = 02/13/15 Pct Recovery = 52% Analysis Date = 02/13/15 Pct Recovery = 52% Analysis Date = 02/08/15 Pct Recovery = 52% Analysis Date = 02/08/15 Pct Recovery = 52% Analysis Date = 02/04/15 Pct Recovery = 52% Analysis Date = 02/04/15 Pct Recovery = 52% Analysis Date = 01/30/15 Pct Recovery = 52% Analysis Date = 01/30/15 Pct Recovery = 52% Analysis Date = 01/25/15 Pct Recovery = 52% Analysis Date = 01/25/15 Pct Recovery = 52% Analysis Date = 01/20/15 Pct Recovery = 52% Analysis Date = 01/20/15 Pct Recovery = 52% Analysis Date = 01/15/15 Pct Recovery = 52% Analysis Date = 01/15/15 Pct Recovery = 52% Analysis Date = 01/11/15 Pct Recovery = 52% Analysis Date = 01/11/15 Pct Recovery = 52% Analysis Date = 01/06/15 Pct Recovery = 52% Analysis Date = 01/06/15 Pct Recovery = 52% Analysis Date = 01/01/15 Pct Recovery = 52% Analysis Date = 01/01/15 Pct Recovery = 52% Analysis Date = 12/27/14 Pct Recovery = 52% Analysis Date = 12/27/14 Pct Recovery = 52% Analysis Date = 12/22/14 Pct Recovery = 52% Analysis Date = 12/22/14 Pct Recovery = 52% Analysis Date = 12/18/14 Pct Recovery = 52% Analysis Date = 12/18/14 Pct Recovery = 52% Analysis Date = 12/13/14 Pct Recovery = 51% Analysis Date = 12/13/14 Pct Recovery = 51% Analysis Date = 12/08/14 Pct Recovery = 51% Analysis Date = 12/08/14 Pct Recovery = 51% Analysis Date = 12/03/14 Pct Recovery = 51% Analysis Date = 12/03/14 Pct Recovery = 51% Analysis Date = 11/28/14 Pct Recovery = 51% Analysis Date = 11/28/14 Pct Recovery = 51% Analysis Date = 11/24/14 Pct Recovery = 51% Analysis Date = 11/24/14 Pct Recovery = 51% Analysis Date = 11/19/14 Pct Recovery = 51% Analysis Date = 11/19/14 Pct Recovery = 51% Analysis Date = 11/14/14 Pct Recovery = 51% Analysis Date = 11/14/14 Pct Recovery = 51% Analysis Date = 11/09/14 Pct Recovery = 51% Analysis Date = 11/09/14 Pct Recovery = 51% Analysis Date = 11/04/14 Pct Recovery = 51% Analysis Date = 11/04/14 Pct Recovery = 51% Analysis Date = 10/31/14 Pct Recovery = 51% Analysis Date = 10/31/14 Pct Recovery = 51% Analysis Date = 10/26/14 Pct Recovery = 51% Analysis Date = 10/26/14 Pct Recovery = 51% Analysis Date = 10/21/14 Pct Recovery = 51% Analysis Date = 10/21/14 Pct Recovery = 51% Analysis Date = 10/16/14 Pct Recovery = 51% Analysis Date = 10/16/14 Pct Recovery = 51% Analysis Date = 10/11/14 Pct Recovery = 51% Analysis Date = 10/11/14 Pct Recovery = 51% Analysis Date = 10/07/14 Pct Recovery = 51% Analysis Date = 10/07/14 Pct Recovery = 51% Analysis Date = 10/02/14 Pct Recovery = 51% Analysis Date = 10/02/14 Pct Recovery = 51% Analysis Date = 09/27/14 Pct Recovery = 51% Analysis Date = 09/27/14 Pct Recovery = 51% Analysis Date = 09/22/14 Pct Recovery = 51% Analysis Date = 09/22/14 Pct Recovery = 51% Analysis Date = 09/17/14 Pct Recovery = 51% Analysis Date = 09/17/14 Pct Recovery = 51% Analysis Date = 09/13/14 Pct Recovery = 51% Analysis Date = 09/13/14 Pct Recovery = 51% Analysis Date = 09/08/14 Pct Recovery = 51% Analysis Date = 09/08/14 Pct Recovery = 51% Analysis Date = 09/03/14 Pct Recovery = 51% Analysis Date = 09/03/14 Pct Recovery = 51% Analysis Date = 08/29/14 Pct Recovery = 51% Analysis Date = 08/29/14 Pct Recovery = 51% Analysis Date = 08/24/14 Pct Recovery = 51% Analysis Date = 08/24/14 Pct Recovery = 51% Analysis Date = 08/20/14 Pct Recovery = 51% Analysis Date = 08/20/14 Pct Recovery = 51% Analysis Date = 08/15/14 Pct Recovery = 51% Analysis Date = 08/15/14 Pct Recovery = 51% Analysis Date = 08/10/14 Pct Recovery = 51% Analysis Date = 08/10/14 Pct Recovery = 51% Analysis Date = 08/05/14 Pct Recovery = 51% Analysis Date = 08/05/14 Pct Recovery = 51% Analysis Date = 07/31/14 Pct Recovery = 51% Analysis Date = 07/31/14 Pct Recovery = 51% Analysis Date = 07/27/14 Pct Recovery = 51% Analysis Date = 07/27/14 Pct Recovery = 51% Analysis Date = 07/22/14 Pct Recovery = 51% Analysis Date = 07/22/14 Pct Recovery = 51% Analysis Date = 07/17/14 Pct Recovery = 51% Analysis Date = 07/17/14 Pct Recovery = 51% Analysis Date = 07/12/14 Pct Recovery = 51% Analysis Date = 07/12/14 Pct Recovery = 51% Analysis Date = 07/07/14 Pct Recovery = 51% Analysis Date = 07/07/14 Pct Recovery = 51% Analysis Date = 07/03/14 Pct Recovery = 51% Analysis Date = 07/03/14 Pct Recovery = 51% Analysis Date = 06/28/14 Pct Recovery = 51% Analysis Date = 06/28/14 Pct Recovery = 51% Analysis Date = 06/23/14 Pct Recovery = 51% Analysis Date = 06/23/14 Pct Recovery = 51% Analysis Date = 06/18/14 Pct Recovery = 51% Analysis Date = 06/18/14 Pct Recovery = 51% Analysis Date = 06/13/14 Pct Recovery = 51% Analysis Date = 06/13/14 Pct Recovery = 51% Analysis Date = 06/09/14 Pct Recovery = 51% Analysis Date = 06/09/14 Pct Recovery = 51% Analysis Date = 06/04/14 Pct Recovery = 51% Analysis Date = 06/04/14 Pct Recovery = 51% Analysis Date = 05/30/14 Pct Recovery = 51% Analysis Date = 05/30/14 Pct Recovery = 51% Analysis Date = 05/25/14 Pct Recovery = 51% Analysis Date = 05/25/14 Pct Recovery = 51% Analysis Date = 05/21/14 Pct Recovery = 51% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
AMITRIPTYLINE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 2 27% 21% 27% 22%
>= Reporting Level 73 55% 14% 56% 13%
Total 75 54% 14% 55% 14%

Sample Statistics
AMITRIPTYLINE

Characteristic N % % Basis
Plotted 75 100% Spiked
Estimated Values 75 100% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 75 .  
False Negatives 0 0% 0 out of 75
Not Spiked 40 .  
False Positives 0 0% 0 out of 40

BQS OBSP Determination:
AMPHETAMINE
METHOD: 2440 , TESTIDCODE: 67461LCM56
Open Data Set

Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 76% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 78% Analysis Date = 11/24/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 82% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 80 µl & Abs 051315: 80 µl Pct Recovery = 69% Analysis Date = 10/01/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 74% Analysis Date = 09/24/16 SpikeMix = Crescent EN160610015: 80 µl & Abs 061416: 80 µl Pct Recovery = 76% Analysis Date = 09/24/16 SpikeMix = Abs 061416: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 72% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 83% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 79% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 80% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 80% Analysis Date = 11/18/16 SpikeMix = ERA 04281604: 80 µl & ERA 04281603: 80 µl Pct Recovery = 81% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & ERA 04281604: 80 µl Pct Recovery = 79% Analysis Date = 05/07/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 92% Analysis Date = 03/11/15 SpikeMix = ERA 0318-14-02: 15 µl & Abs 041714: 15 µl Pct Recovery = 82% Analysis Date = 01/16/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 86% Analysis Date = 12/06/14 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 72% Analysis Date = 08/21/14 SpikeMix = ERA 0318-14-02: 60 µl & Abs 041714: 60 µl Pct Recovery = 70% Analysis Date = 07/12/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 67% Analysis Date = 06/11/14 SpikeMix = Abs 041614: 60 µl & Abs 041714: 60 µl Pct Recovery = 76% Analysis Date = 05/21/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 72% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 77% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 67% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-07A: 40 µl & Abs 051315: 40 µl Pct Recovery = 65% Analysis Date = 07/31/15 SpikeMix = Abs 051315: 40 µl & Abs 052215: 40 µl Pct Recovery = 74% Analysis Date = 07/30/15 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 88% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 83% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 67% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 69% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 67% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 58% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 66% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 56% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 63% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 116% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 102% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 89% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 92% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 78% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 76% Analysis Date = 11/04/14 SpikeMix = Abs 041714: 8 µl & ERA 0319-14-05: 8 µl Pct Recovery = 62% Analysis Date = 10/10/14 SpikeMix = Abs 041714: 30 µl & Abs 041814: 30 µl Pct Recovery = 70% Analysis Date = 07/20/14 SpikeMix = ERA 0318-14-02: 30 µl & Abs 041714: 30 µl Pct Recovery = 49% Analysis Date = 06/28/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 73% Analysis Date = 05/17/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 67% Analysis Date = 02/23/16 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 58% Analysis Date = 08/11/15 SpikeMix = Abs 050115: 20 µl & Abs 051315: 20 µl Pct Recovery = 81% Analysis Date = 06/26/15 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 65% Analysis Date = 06/09/15 SpikeMix = Abs 051315: 20 µl & Abs 050115: 20 µl Pct Recovery = 76% Analysis Date = 04/09/16 SpikeMix = Abs 051315: 10 µl & ERA 0406-15-09: 10 µl Pct Recovery = 71% Analysis Date = 01/04/17 Pct Recovery = 88% Analysis Date = 12/31/16 Pct Recovery = 88% Analysis Date = 12/31/16 Pct Recovery = 88% Analysis Date = 12/26/16 Pct Recovery = 87% Analysis Date = 12/26/16 Pct Recovery = 87% Analysis Date = 12/21/16 Pct Recovery = 87% Analysis Date = 12/21/16 Pct Recovery = 87% Analysis Date = 12/16/16 Pct Recovery = 86% Analysis Date = 12/16/16 Pct Recovery = 86% Analysis Date = 12/11/16 Pct Recovery = 86% Analysis Date = 12/11/16 Pct Recovery = 86% Analysis Date = 12/07/16 Pct Recovery = 85% Analysis Date = 12/07/16 Pct Recovery = 85% Analysis Date = 12/02/16 Pct Recovery = 85% Analysis Date = 12/02/16 Pct Recovery = 85% Analysis Date = 11/27/16 Pct Recovery = 84% Analysis Date = 11/27/16 Pct Recovery = 84% Analysis Date = 11/22/16 Pct Recovery = 84% Analysis Date = 11/22/16 Pct Recovery = 84% Analysis Date = 11/17/16 Pct Recovery = 83% Analysis Date = 11/17/16 Pct Recovery = 83% Analysis Date = 11/12/16 Pct Recovery = 83% Analysis Date = 11/12/16 Pct Recovery = 83% Analysis Date = 11/08/16 Pct Recovery = 82% Analysis Date = 11/08/16 Pct Recovery = 82% Analysis Date = 11/03/16 Pct Recovery = 82% Analysis Date = 11/03/16 Pct Recovery = 82% Analysis Date = 10/29/16 Pct Recovery = 81% Analysis Date = 10/29/16 Pct Recovery = 81% Analysis Date = 10/24/16 Pct Recovery = 81% Analysis Date = 10/24/16 Pct Recovery = 81% Analysis Date = 10/19/16 Pct Recovery = 80% Analysis Date = 10/19/16 Pct Recovery = 80% Analysis Date = 10/15/16 Pct Recovery = 80% Analysis Date = 10/15/16 Pct Recovery = 80% Analysis Date = 10/10/16 Pct Recovery = 79% Analysis Date = 10/10/16 Pct Recovery = 79% Analysis Date = 10/05/16 Pct Recovery = 79% Analysis Date = 10/05/16 Pct Recovery = 79% Analysis Date = 09/30/16 Pct Recovery = 78% Analysis Date = 09/30/16 Pct Recovery = 78% Analysis Date = 09/25/16 Pct Recovery = 78% Analysis Date = 09/25/16 Pct Recovery = 78% Analysis Date = 09/20/16 Pct Recovery = 77% Analysis Date = 09/20/16 Pct Recovery = 77% Analysis Date = 09/16/16 Pct Recovery = 77% Analysis Date = 09/16/16 Pct Recovery = 77% Analysis Date = 09/11/16 Pct Recovery = 76% Analysis Date = 09/11/16 Pct Recovery = 76% Analysis Date = 09/06/16 Pct Recovery = 76% Analysis Date = 09/06/16 Pct Recovery = 76% Analysis Date = 09/01/16 Pct Recovery = 76% Analysis Date = 09/01/16 Pct Recovery = 76% Analysis Date = 08/27/16 Pct Recovery = 75% Analysis Date = 08/27/16 Pct Recovery = 75% Analysis Date = 08/23/16 Pct Recovery = 75% Analysis Date = 08/23/16 Pct Recovery = 75% Analysis Date = 08/18/16 Pct Recovery = 74% Analysis Date = 08/18/16 Pct Recovery = 74% Analysis Date = 08/13/16 Pct Recovery = 74% Analysis Date = 08/13/16 Pct Recovery = 74% Analysis Date = 08/08/16 Pct Recovery = 74% Analysis Date = 08/08/16 Pct Recovery = 74% Analysis Date = 08/03/16 Pct Recovery = 73% Analysis Date = 08/03/16 Pct Recovery = 73% Analysis Date = 07/29/16 Pct Recovery = 73% Analysis Date = 07/29/16 Pct Recovery = 73% Analysis Date = 07/25/16 Pct Recovery = 72% Analysis Date = 07/25/16 Pct Recovery = 72% Analysis Date = 07/20/16 Pct Recovery = 72% Analysis Date = 07/20/16 Pct Recovery = 72% Analysis Date = 07/15/16 Pct Recovery = 72% Analysis Date = 07/15/16 Pct Recovery = 72% Analysis Date = 07/10/16 Pct Recovery = 72% Analysis Date = 07/10/16 Pct Recovery = 72% Analysis Date = 07/05/16 Pct Recovery = 72% Analysis Date = 07/05/16 Pct Recovery = 72% Analysis Date = 07/01/16 Pct Recovery = 72% Analysis Date = 07/01/16 Pct Recovery = 72% Analysis Date = 06/26/16 Pct Recovery = 72% Analysis Date = 06/26/16 Pct Recovery = 72% Analysis Date = 06/21/16 Pct Recovery = 72% Analysis Date = 06/21/16 Pct Recovery = 72% Analysis Date = 06/16/16 Pct Recovery = 71% Analysis Date = 06/16/16 Pct Recovery = 71% Analysis Date = 06/11/16 Pct Recovery = 71% Analysis Date = 06/11/16 Pct Recovery = 71% Analysis Date = 06/06/16 Pct Recovery = 71% Analysis Date = 06/06/16 Pct Recovery = 71% Analysis Date = 06/02/16 Pct Recovery = 71% Analysis Date = 06/02/16 Pct Recovery = 71% Analysis Date = 05/28/16 Pct Recovery = 71% Analysis Date = 05/28/16 Pct Recovery = 71% Analysis Date = 05/23/16 Pct Recovery = 71% Analysis Date = 05/23/16 Pct Recovery = 71% Analysis Date = 05/18/16 Pct Recovery = 71% Analysis Date = 05/18/16 Pct Recovery = 71% Analysis Date = 05/13/16 Pct Recovery = 71% Analysis Date = 05/13/16 Pct Recovery = 71% Analysis Date = 05/08/16 Pct Recovery = 71% Analysis Date = 05/08/16 Pct Recovery = 71% Analysis Date = 05/04/16 Pct Recovery = 70% Analysis Date = 05/04/16 Pct Recovery = 70% Analysis Date = 04/29/16 Pct Recovery = 70% Analysis Date = 04/29/16 Pct Recovery = 70% Analysis Date = 04/24/16 Pct Recovery = 70% Analysis Date = 04/24/16 Pct Recovery = 70% Analysis Date = 04/19/16 Pct Recovery = 70% Analysis Date = 04/19/16 Pct Recovery = 70% Analysis Date = 04/14/16 Pct Recovery = 71% Analysis Date = 04/14/16 Pct Recovery = 71% Analysis Date = 04/10/16 Pct Recovery = 71% Analysis Date = 04/10/16 Pct Recovery = 71% Analysis Date = 04/05/16 Pct Recovery = 71% Analysis Date = 04/05/16 Pct Recovery = 71% Analysis Date = 03/31/16 Pct Recovery = 71% Analysis Date = 03/31/16 Pct Recovery = 71% Analysis Date = 03/26/16 Pct Recovery = 71% Analysis Date = 03/26/16 Pct Recovery = 71% Analysis Date = 03/21/16 Pct Recovery = 71% Analysis Date = 03/21/16 Pct Recovery = 71% Analysis Date = 03/16/16 Pct Recovery = 71% Analysis Date = 03/16/16 Pct Recovery = 71% Analysis Date = 03/12/16 Pct Recovery = 71% Analysis Date = 03/12/16 Pct Recovery = 71% Analysis Date = 03/07/16 Pct Recovery = 71% Analysis Date = 03/07/16 Pct Recovery = 71% Analysis Date = 03/02/16 Pct Recovery = 72% Analysis Date = 03/02/16 Pct Recovery = 72% Analysis Date = 02/26/16 Pct Recovery = 72% Analysis Date = 02/26/16 Pct Recovery = 72% Analysis Date = 02/21/16 Pct Recovery = 72% Analysis Date = 02/21/16 Pct Recovery = 72% Analysis Date = 02/17/16 Pct Recovery = 72% Analysis Date = 02/17/16 Pct Recovery = 72% Analysis Date = 02/12/16 Pct Recovery = 72% Analysis Date = 02/12/16 Pct Recovery = 72% Analysis Date = 02/07/16 Pct Recovery = 72% Analysis Date = 02/07/16 Pct Recovery = 72% Analysis Date = 02/02/16 Pct Recovery = 72% Analysis Date = 02/02/16 Pct Recovery = 72% Analysis Date = 01/28/16 Pct Recovery = 72% Analysis Date = 01/28/16 Pct Recovery = 72% Analysis Date = 01/23/16 Pct Recovery = 72% Analysis Date = 01/23/16 Pct Recovery = 72% Analysis Date = 01/19/16 Pct Recovery = 72% Analysis Date = 01/19/16 Pct Recovery = 72% Analysis Date = 01/14/16 Pct Recovery = 73% Analysis Date = 01/14/16 Pct Recovery = 73% Analysis Date = 01/09/16 Pct Recovery = 73% Analysis Date = 01/09/16 Pct Recovery = 73% Analysis Date = 01/04/16 Pct Recovery = 73% Analysis Date = 01/04/16 Pct Recovery = 73% Analysis Date = 12/30/15 Pct Recovery = 73% Analysis Date = 12/30/15 Pct Recovery = 73% Analysis Date = 12/26/15 Pct Recovery = 73% Analysis Date = 12/26/15 Pct Recovery = 73% Analysis Date = 12/21/15 Pct Recovery = 73% Analysis Date = 12/21/15 Pct Recovery = 73% Analysis Date = 12/16/15 Pct Recovery = 73% Analysis Date = 12/16/15 Pct Recovery = 73% Analysis Date = 12/11/15 Pct Recovery = 73% Analysis Date = 12/11/15 Pct Recovery = 73% Analysis Date = 12/06/15 Pct Recovery = 73% Analysis Date = 12/06/15 Pct Recovery = 73% Analysis Date = 12/01/15 Pct Recovery = 74% Analysis Date = 12/01/15 Pct Recovery = 74% Analysis Date = 11/27/15 Pct Recovery = 74% Analysis Date = 11/27/15 Pct Recovery = 74% Analysis Date = 11/22/15 Pct Recovery = 74% Analysis Date = 11/22/15 Pct Recovery = 74% Analysis Date = 11/17/15 Pct Recovery = 74% Analysis Date = 11/17/15 Pct Recovery = 74% Analysis Date = 11/12/15 Pct Recovery = 74% Analysis Date = 11/12/15 Pct Recovery = 74% Analysis Date = 11/07/15 Pct Recovery = 74% Analysis Date = 11/07/15 Pct Recovery = 74% Analysis Date = 11/03/15 Pct Recovery = 74% Analysis Date = 11/03/15 Pct Recovery = 74% Analysis Date = 10/29/15 Pct Recovery = 74% Analysis Date = 10/29/15 Pct Recovery = 74% Analysis Date = 10/24/15 Pct Recovery = 74% Analysis Date = 10/24/15 Pct Recovery = 74% Analysis Date = 10/19/15 Pct Recovery = 74% Analysis Date = 10/19/15 Pct Recovery = 74% Analysis Date = 10/14/15 Pct Recovery = 75% Analysis Date = 10/14/15 Pct Recovery = 75% Analysis Date = 10/09/15 Pct Recovery = 75% Analysis Date = 10/09/15 Pct Recovery = 75% Analysis Date = 10/05/15 Pct Recovery = 75% Analysis Date = 10/05/15 Pct Recovery = 75% Analysis Date = 09/30/15 Pct Recovery = 75% Analysis Date = 09/30/15 Pct Recovery = 75% Analysis Date = 09/25/15 Pct Recovery = 75% Analysis Date = 09/25/15 Pct Recovery = 75% Analysis Date = 09/20/15 Pct Recovery = 75% Analysis Date = 09/20/15 Pct Recovery = 75% Analysis Date = 09/15/15 Pct Recovery = 75% Analysis Date = 09/15/15 Pct Recovery = 75% Analysis Date = 09/10/15 Pct Recovery = 75% Analysis Date = 09/10/15 Pct Recovery = 75% Analysis Date = 09/06/15 Pct Recovery = 75% Analysis Date = 09/06/15 Pct Recovery = 75% Analysis Date = 09/01/15 Pct Recovery = 75% Analysis Date = 09/01/15 Pct Recovery = 75% Analysis Date = 08/27/15 Pct Recovery = 75% Analysis Date = 08/27/15 Pct Recovery = 75% Analysis Date = 08/22/15 Pct Recovery = 75% Analysis Date = 08/22/15 Pct Recovery = 75% Analysis Date = 08/17/15 Pct Recovery = 75% Analysis Date = 08/17/15 Pct Recovery = 75% Analysis Date = 08/13/15 Pct Recovery = 75% Analysis Date = 08/13/15 Pct Recovery = 75% Analysis Date = 08/08/15 Pct Recovery = 75% Analysis Date = 08/08/15 Pct Recovery = 75% Analysis Date = 08/03/15 Pct Recovery = 75% Analysis Date = 08/03/15 Pct Recovery = 75% Analysis Date = 07/29/15 Pct Recovery = 75% Analysis Date = 07/29/15 Pct Recovery = 75% Analysis Date = 07/24/15 Pct Recovery = 75% Analysis Date = 07/24/15 Pct Recovery = 75% Analysis Date = 07/19/15 Pct Recovery = 75% Analysis Date = 07/19/15 Pct Recovery = 75% Analysis Date = 07/15/15 Pct Recovery = 75% Analysis Date = 07/15/15 Pct Recovery = 75% Analysis Date = 07/10/15 Pct Recovery = 75% Analysis Date = 07/10/15 Pct Recovery = 75% Analysis Date = 07/05/15 Pct Recovery = 75% Analysis Date = 07/05/15 Pct Recovery = 75% Analysis Date = 06/30/15 Pct Recovery = 75% Analysis Date = 06/30/15 Pct Recovery = 75% Analysis Date = 06/25/15 Pct Recovery = 75% Analysis Date = 06/25/15 Pct Recovery = 75% Analysis Date = 06/21/15 Pct Recovery = 75% Analysis Date = 06/21/15 Pct Recovery = 75% Analysis Date = 06/16/15 Pct Recovery = 75% Analysis Date = 06/16/15 Pct Recovery = 75% Analysis Date = 06/11/15 Pct Recovery = 75% Analysis Date = 06/11/15 Pct Recovery = 75% Analysis Date = 06/06/15 Pct Recovery = 75% Analysis Date = 06/06/15 Pct Recovery = 75% Analysis Date = 06/01/15 Pct Recovery = 75% Analysis Date = 06/01/15 Pct Recovery = 75% Analysis Date = 05/27/15 Pct Recovery = 75% Analysis Date = 05/27/15 Pct Recovery = 75% Analysis Date = 05/23/15 Pct Recovery = 75% Analysis Date = 05/23/15 Pct Recovery = 75% Analysis Date = 05/18/15 Pct Recovery = 75% Analysis Date = 05/18/15 Pct Recovery = 75% Analysis Date = 05/13/15 Pct Recovery = 75% Analysis Date = 05/13/15 Pct Recovery = 75% Analysis Date = 05/08/15 Pct Recovery = 75% Analysis Date = 05/08/15 Pct Recovery = 75% Analysis Date = 05/03/15 Pct Recovery = 74% Analysis Date = 05/03/15 Pct Recovery = 74% Analysis Date = 04/29/15 Pct Recovery = 74% Analysis Date = 04/29/15 Pct Recovery = 74% Analysis Date = 04/24/15 Pct Recovery = 74% Analysis Date = 04/24/15 Pct Recovery = 74% Analysis Date = 04/19/15 Pct Recovery = 74% Analysis Date = 04/19/15 Pct Recovery = 74% Analysis Date = 04/14/15 Pct Recovery = 74% Analysis Date = 04/14/15 Pct Recovery = 74% Analysis Date = 04/09/15 Pct Recovery = 74% Analysis Date = 04/09/15 Pct Recovery = 74% Analysis Date = 04/04/15 Pct Recovery = 74% Analysis Date = 04/04/15 Pct Recovery = 74% Analysis Date = 03/31/15 Pct Recovery = 74% Analysis Date = 03/31/15 Pct Recovery = 74% Analysis Date = 03/26/15 Pct Recovery = 74% Analysis Date = 03/26/15 Pct Recovery = 74% Analysis Date = 03/21/15 Pct Recovery = 74% Analysis Date = 03/21/15 Pct Recovery = 74% Analysis Date = 03/16/15 Pct Recovery = 74% Analysis Date = 03/16/15 Pct Recovery = 74% Analysis Date = 03/11/15 Pct Recovery = 74% Analysis Date = 03/11/15 Pct Recovery = 74% Analysis Date = 03/07/15 Pct Recovery = 73% Analysis Date = 03/07/15 Pct Recovery = 73% Analysis Date = 03/02/15 Pct Recovery = 73% Analysis Date = 03/02/15 Pct Recovery = 73% Analysis Date = 02/25/15 Pct Recovery = 73% Analysis Date = 02/25/15 Pct Recovery = 73% Analysis Date = 02/20/15 Pct Recovery = 73% Analysis Date = 02/20/15 Pct Recovery = 73% Analysis Date = 02/15/15 Pct Recovery = 73% Analysis Date = 02/15/15 Pct Recovery = 73% Analysis Date = 02/10/15 Pct Recovery = 73% Analysis Date = 02/10/15 Pct Recovery = 73% Analysis Date = 02/06/15 Pct Recovery = 73% Analysis Date = 02/06/15 Pct Recovery = 73% Analysis Date = 02/01/15 Pct Recovery = 73% Analysis Date = 02/01/15 Pct Recovery = 73% Analysis Date = 01/27/15 Pct Recovery = 73% Analysis Date = 01/27/15 Pct Recovery = 73% Analysis Date = 01/22/15 Pct Recovery = 73% Analysis Date = 01/22/15 Pct Recovery = 73% Analysis Date = 01/17/15 Pct Recovery = 73% Analysis Date = 01/17/15 Pct Recovery = 73% Analysis Date = 01/12/15 Pct Recovery = 73% Analysis Date = 01/12/15 Pct Recovery = 73% Analysis Date = 01/08/15 Pct Recovery = 72% Analysis Date = 01/08/15 Pct Recovery = 72% Analysis Date = 01/03/15 Pct Recovery = 72% Analysis Date = 01/03/15 Pct Recovery = 72% Analysis Date = 12/29/14 Pct Recovery = 72% Analysis Date = 12/29/14 Pct Recovery = 72% Analysis Date = 12/24/14 Pct Recovery = 72% Analysis Date = 12/24/14 Pct Recovery = 72% Analysis Date = 12/19/14 Pct Recovery = 72% Analysis Date = 12/19/14 Pct Recovery = 72% Analysis Date = 12/15/14 Pct Recovery = 72% Analysis Date = 12/15/14 Pct Recovery = 72% Analysis Date = 12/10/14 Pct Recovery = 72% Analysis Date = 12/10/14 Pct Recovery = 72% Analysis Date = 12/05/14 Pct Recovery = 72% Analysis Date = 12/05/14 Pct Recovery = 72% Analysis Date = 11/30/14 Pct Recovery = 72% Analysis Date = 11/30/14 Pct Recovery = 72% Analysis Date = 11/25/14 Pct Recovery = 72% Analysis Date = 11/25/14 Pct Recovery = 72% Analysis Date = 11/20/14 Pct Recovery = 72% Analysis Date = 11/20/14 Pct Recovery = 72% Analysis Date = 11/16/14 Pct Recovery = 72% Analysis Date = 11/16/14 Pct Recovery = 72% Analysis Date = 11/11/14 Pct Recovery = 72% Analysis Date = 11/11/14 Pct Recovery = 72% Analysis Date = 11/06/14 Pct Recovery = 71% Analysis Date = 11/06/14 Pct Recovery = 71% Analysis Date = 11/01/14 Pct Recovery = 71% Analysis Date = 11/01/14 Pct Recovery = 71% Analysis Date = 10/27/14 Pct Recovery = 71% Analysis Date = 10/27/14 Pct Recovery = 71% Analysis Date = 10/23/14 Pct Recovery = 71% Analysis Date = 10/23/14 Pct Recovery = 71% Analysis Date = 10/18/14 Pct Recovery = 71% Analysis Date = 10/18/14 Pct Recovery = 71% Analysis Date = 10/13/14 Pct Recovery = 71% Analysis Date = 10/13/14 Pct Recovery = 71% Analysis Date = 10/08/14 Pct Recovery = 71% Analysis Date = 10/08/14 Pct Recovery = 71% Analysis Date = 10/03/14 Pct Recovery = 71% Analysis Date = 10/03/14 Pct Recovery = 71% Analysis Date = 09/28/14 Pct Recovery = 71% Analysis Date = 09/28/14 Pct Recovery = 71% Analysis Date = 09/24/14 Pct Recovery = 71% Analysis Date = 09/24/14 Pct Recovery = 71% Analysis Date = 09/19/14 Pct Recovery = 71% Analysis Date = 09/19/14 Pct Recovery = 71% Analysis Date = 09/14/14 Pct Recovery = 71% Analysis Date = 09/14/14 Pct Recovery = 71% Analysis Date = 09/09/14 Pct Recovery = 70% Analysis Date = 09/09/14 Pct Recovery = 70% Analysis Date = 09/04/14 Pct Recovery = 70% Analysis Date = 09/04/14 Pct Recovery = 70% Analysis Date = 08/31/14 Pct Recovery = 70% Analysis Date = 08/31/14 Pct Recovery = 70% Analysis Date = 08/26/14 Pct Recovery = 70% Analysis Date = 08/26/14 Pct Recovery = 70% Analysis Date = 08/21/14 Pct Recovery = 70% Analysis Date = 08/21/14 Pct Recovery = 70% Analysis Date = 08/16/14 Pct Recovery = 70% Analysis Date = 08/16/14 Pct Recovery = 70% Analysis Date = 08/11/14 Pct Recovery = 70% Analysis Date = 08/11/14 Pct Recovery = 70% Analysis Date = 08/06/14 Pct Recovery = 70% Analysis Date = 08/06/14 Pct Recovery = 70% Analysis Date = 08/02/14 Pct Recovery = 70% Analysis Date = 08/02/14 Pct Recovery = 70% Analysis Date = 07/28/14 Pct Recovery = 70% Analysis Date = 07/28/14 Pct Recovery = 70% Analysis Date = 07/23/14 Pct Recovery = 70% Analysis Date = 07/23/14 Pct Recovery = 70% Analysis Date = 07/18/14 Pct Recovery = 69% Analysis Date = 07/18/14 Pct Recovery = 69% Analysis Date = 07/13/14 Pct Recovery = 69% Analysis Date = 07/13/14 Pct Recovery = 69% Analysis Date = 07/09/14 Pct Recovery = 69% Analysis Date = 07/09/14 Pct Recovery = 69% Analysis Date = 07/04/14 Pct Recovery = 69% Analysis Date = 07/04/14 Pct Recovery = 69% Analysis Date = 06/29/14 Pct Recovery = 69% Analysis Date = 06/29/14 Pct Recovery = 69% Analysis Date = 06/24/14 Pct Recovery = 69% Analysis Date = 06/24/14 Pct Recovery = 69% Analysis Date = 06/19/14 Pct Recovery = 69% Analysis Date = 06/19/14 Pct Recovery = 69% Analysis Date = 06/14/14 Pct Recovery = 69% Analysis Date = 06/14/14 Pct Recovery = 69% Analysis Date = 06/10/14 Pct Recovery = 69% Analysis Date = 06/10/14 Pct Recovery = 69% Analysis Date = 06/05/14 Pct Recovery = 68% Analysis Date = 06/05/14 Pct Recovery = 68% Analysis Date = 05/31/14 Pct Recovery = 68% Analysis Date = 05/31/14 Pct Recovery = 68% Analysis Date = 05/26/14 Pct Recovery = 68% Analysis Date = 05/26/14 Pct Recovery = 68% Analysis Date = 05/21/14 Pct Recovery = 68% Analysis Date = 05/21/14 Pct Recovery = 68% Analysis Date = 05/17/14 Pct Recovery = 68% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
AMPHETAMINE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 1 71% . 71% 0%
>= Reporting Level 49 75% 12% 76% 10%
Total 50 75% 12% 75% 10%

Sample Statistics
AMPHETAMINE

Characteristic N % % Basis
Plotted 50 98% Spiked
Estimated Values 11 22% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 1 2% Spiked
Spiked 51 .  
False Negatives 0 0% 0 out of 51
Not Spiked 64 .  
False Positives 0 0% 0 out of 64

BQS OBSP Determination:
ANTIPYRENE
METHOD: 2440 , TESTIDCODE: 67477LCM56
Open Data Set

Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 97% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 90% Analysis Date = 11/05/15 SpikeMix = ERA 0406-15-08: 80 µl & Abs 052215: 80 µl Pct Recovery = 81% Analysis Date = 11/04/15 SpikeMix = Abs 052215: 80 µl & Abs 050115: 80 µl Pct Recovery = 76% Analysis Date = 01/17/16 SpikeMix = ERA 0406-15-09: 80 µl & ERA 0406-15-07A: 80 µl Pct Recovery = 76% Analysis Date = 11/24/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 81% Analysis Date = 10/01/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 75% Analysis Date = 11/18/16 SpikeMix = ERA 04281604: 80 µl & ERA 04281603: 80 µl Pct Recovery = 79% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & ERA 04281604: 80 µl Pct Recovery = 79% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 73% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 73% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 78% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 80% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 89% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 90% Analysis Date = 05/07/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 97% Analysis Date = 04/29/15 SpikeMix = ERA 0319-14-05: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 100% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 88% Analysis Date = 01/16/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 78% Analysis Date = 12/07/14 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 78% Analysis Date = 12/06/14 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 72% Analysis Date = 08/28/14 SpikeMix = ERA 0319-14-04: 60 µl & ERA 0319-14-05: 60 µl Pct Recovery = 61% Analysis Date = 07/26/14 SpikeMix = ERA 0319-14-05: 60 µl & ERA 0318-14-02: 60 µl Pct Recovery = 88% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-04: 15 µl & Abs 041814: 15 µl Pct Recovery = 78% Analysis Date = 02/06/15 SpikeMix = Abs 041814: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 84% Analysis Date = 07/12/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 85% Analysis Date = 06/22/14 SpikeMix = Abs 041814: 60 µl & Abs 041614: 60 µl Pct Recovery = 95% Analysis Date = 05/21/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 90% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-08: 40 µl & Abs 052215: 40 µl Pct Recovery = 76% Analysis Date = 02/23/16 SpikeMix = Abs 052215: 40 µl & Abs 050115: 40 µl Pct Recovery = 73% Analysis Date = 09/10/15 SpikeMix = Abs 052215: 40 µl & ERA 0406-15-07A: 40 µl Pct Recovery = 97% Analysis Date = 07/31/15 SpikeMix = Abs 051315: 40 µl & Abs 052215: 40 µl Pct Recovery = 72% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-08: 40 µl & ERA 0406-15-09: 40 µl Pct Recovery = 76% Analysis Date = 07/31/15 SpikeMix = ERA 0406-15-09: 40 µl & Abs 050115: 40 µl Pct Recovery = 96% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 70% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 84% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 67% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 68% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 102% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 117% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 90% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 86% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 80% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 79% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 69% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 77% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 72% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 61% Analysis Date = 11/04/14 SpikeMix = Abs 041714: 8 µl & ERA 0319-14-05: 8 µl Pct Recovery = 69% Analysis Date = 10/24/14 SpikeMix = ERA 0319-14-05: 8 µl & Abs 041614: 8 µl Pct Recovery = 75% Analysis Date = 04/10/15 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 89% Analysis Date = 11/04/14 SpikeMix = Abs 041814: 8 µl & ERA 0318-14-02: 8 µl Pct Recovery = 81% Analysis Date = 10/11/14 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 65% Analysis Date = 08/30/14 SpikeMix = ERA 0318-14-02: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 82% Analysis Date = 08/16/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 41% Analysis Date = 07/13/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 90% Analysis Date = 10/10/14 SpikeMix = Abs 041714: 30 µl & Abs 041814: 30 µl Pct Recovery = 77% Analysis Date = 10/10/14 SpikeMix = Abs 041814: 30 µl & ERA 0318-14-02: 30 µl Pct Recovery = 69% Analysis Date = 07/13/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 90% Analysis Date = 05/30/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 86% Analysis Date = 04/23/14 SpikeMix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.2: 20 µl Pct Recovery = 82% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 63% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 66% Analysis Date = 02/23/16 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 81% Analysis Date = 11/24/15 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 83% Analysis Date = 09/09/15 SpikeMix = ERA 0406-15-08: 20 µl & Abs 052215: 20 µl Pct Recovery = 84% Analysis Date = 08/27/15 SpikeMix = Abs 052215: 20 µl & Abs 050115: 20 µl Pct Recovery = 79% Analysis Date = 07/09/15 SpikeMix = Abs 050115: 20 µl & Abs 052215: 20 µl Pct Recovery = 77% Analysis Date = 06/26/15 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 78% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 78% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 73% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-08: 20 µl & ERA 0406-15-09: 20 µl Pct Recovery = 74% Analysis Date = 11/24/15 SpikeMix = ERA 0406-15-09: 20 µl & Abs 050115: 20 µl Pct Recovery = 78% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-09: 20 µl Pct Recovery = 58% Analysis Date = 04/09/16 SpikeMix = Abs 051315: 10 µl & ERA 0406-15-09: 10 µl Pct Recovery = 55% Analysis Date = 04/09/16 SpikeMix = Abs 051315: 10 µl & ERA 0406-15-09: 10 µl Pct Recovery = 81% Analysis Date = 01/18/17 Pct Recovery = 88% Analysis Date = 01/13/17 Pct Recovery = 88% Analysis Date = 01/13/17 Pct Recovery = 88% Analysis Date = 01/08/17 Pct Recovery = 87% Analysis Date = 01/08/17 Pct Recovery = 87% Analysis Date = 01/03/17 Pct Recovery = 87% Analysis Date = 01/03/17 Pct Recovery = 87% Analysis Date = 12/29/16 Pct Recovery = 87% Analysis Date = 12/29/16 Pct Recovery = 87% Analysis Date = 12/24/16 Pct Recovery = 86% Analysis Date = 12/24/16 Pct Recovery = 86% Analysis Date = 12/19/16 Pct Recovery = 86% Analysis Date = 12/19/16 Pct Recovery = 86% Analysis Date = 12/14/16 Pct Recovery = 86% Analysis Date = 12/14/16 Pct Recovery = 86% Analysis Date = 12/09/16 Pct Recovery = 85% Analysis Date = 12/09/16 Pct Recovery = 85% Analysis Date = 12/04/16 Pct Recovery = 85% Analysis Date = 12/04/16 Pct Recovery = 85% Analysis Date = 11/29/16 Pct Recovery = 85% Analysis Date = 11/29/16 Pct Recovery = 85% Analysis Date = 11/24/16 Pct Recovery = 84% Analysis Date = 11/24/16 Pct Recovery = 84% Analysis Date = 11/19/16 Pct Recovery = 84% Analysis Date = 11/19/16 Pct Recovery = 84% Analysis Date = 11/14/16 Pct Recovery = 84% Analysis Date = 11/14/16 Pct Recovery = 84% Analysis Date = 11/09/16 Pct Recovery = 83% Analysis Date = 11/09/16 Pct Recovery = 83% Analysis Date = 11/04/16 Pct Recovery = 83% Analysis Date = 11/04/16 Pct Recovery = 83% Analysis Date = 10/30/16 Pct Recovery = 83% Analysis Date = 10/30/16 Pct Recovery = 83% Analysis Date = 10/25/16 Pct Recovery = 82% Analysis Date = 10/25/16 Pct Recovery = 82% Analysis Date = 10/20/16 Pct Recovery = 82% Analysis Date = 10/20/16 Pct Recovery = 82% Analysis Date = 10/15/16 Pct Recovery = 82% Analysis Date = 10/15/16 Pct Recovery = 82% Analysis Date = 10/10/16 Pct Recovery = 81% Analysis Date = 10/10/16 Pct Recovery = 81% Analysis Date = 10/05/16 Pct Recovery = 81% Analysis Date = 10/05/16 Pct Recovery = 81% Analysis Date = 09/30/16 Pct Recovery = 81% Analysis Date = 09/30/16 Pct Recovery = 81% Analysis Date = 09/25/16 Pct Recovery = 81% Analysis Date = 09/25/16 Pct Recovery = 81% Analysis Date = 09/20/16 Pct Recovery = 80% Analysis Date = 09/20/16 Pct Recovery = 80% Analysis Date = 09/15/16 Pct Recovery = 80% Analysis Date = 09/15/16 Pct Recovery = 80% Analysis Date = 09/10/16 Pct Recovery = 80% Analysis Date = 09/10/16 Pct Recovery = 80% Analysis Date = 09/05/16 Pct Recovery = 79% Analysis Date = 09/05/16 Pct Recovery = 79% Analysis Date = 08/31/16 Pct Recovery = 79% Analysis Date = 08/31/16 Pct Recovery = 79% Analysis Date = 08/26/16 Pct Recovery = 79% Analysis Date = 08/26/16 Pct Recovery = 79% Analysis Date = 08/21/16 Pct Recovery = 79% Analysis Date = 08/21/16 Pct Recovery = 79% Analysis Date = 08/16/16 Pct Recovery = 78% Analysis Date = 08/16/16 Pct Recovery = 78% Analysis Date = 08/11/16 Pct Recovery = 78% Analysis Date = 08/11/16 Pct Recovery = 78% Analysis Date = 08/06/16 Pct Recovery = 78% Analysis Date = 08/06/16 Pct Recovery = 78% Analysis Date = 08/01/16 Pct Recovery = 78% Analysis Date = 08/01/16 Pct Recovery = 78% Analysis Date = 07/27/16 Pct Recovery = 78% Analysis Date = 07/27/16 Pct Recovery = 78% Analysis Date = 07/22/16 Pct Recovery = 78% Analysis Date = 07/22/16 Pct Recovery = 78% Analysis Date = 07/17/16 Pct Recovery = 78% Analysis Date = 07/17/16 Pct Recovery = 78% Analysis Date = 07/12/16 Pct Recovery = 78% Analysis Date = 07/12/16 Pct Recovery = 78% Analysis Date = 07/07/16 Pct Recovery = 77% Analysis Date = 07/07/16 Pct Recovery = 77% Analysis Date = 07/02/16 Pct Recovery = 77% Analysis Date = 07/02/16 Pct Recovery = 77% Analysis Date = 06/27/16 Pct Recovery = 77% Analysis Date = 06/27/16 Pct Recovery = 77% Analysis Date = 06/22/16 Pct Recovery = 77% Analysis Date = 06/22/16 Pct Recovery = 77% Analysis Date = 06/17/16 Pct Recovery = 77% Analysis Date = 06/17/16 Pct Recovery = 77% Analysis Date = 06/12/16 Pct Recovery = 77% Analysis Date = 06/12/16 Pct Recovery = 77% Analysis Date = 06/07/16 Pct Recovery = 77% Analysis Date = 06/07/16 Pct Recovery = 77% Analysis Date = 06/02/16 Pct Recovery = 77% Analysis Date = 06/02/16 Pct Recovery = 77% Analysis Date = 05/28/16 Pct Recovery = 76% Analysis Date = 05/28/16 Pct Recovery = 76% Analysis Date = 05/23/16 Pct Recovery = 76% Analysis Date = 05/23/16 Pct Recovery = 76% Analysis Date = 05/18/16 Pct Recovery = 76% Analysis Date = 05/18/16 Pct Recovery = 76% Analysis Date = 05/13/16 Pct Recovery = 76% Analysis Date = 05/13/16 Pct Recovery = 76% Analysis Date = 05/08/16 Pct Recovery = 76% Analysis Date = 05/08/16 Pct Recovery = 76% Analysis Date = 05/03/16 Pct Recovery = 76% Analysis Date = 05/03/16 Pct Recovery = 76% Analysis Date = 04/28/16 Pct Recovery = 76% Analysis Date = 04/28/16 Pct Recovery = 76% Analysis Date = 04/23/16 Pct Recovery = 76% Analysis Date = 04/23/16 Pct Recovery = 76% Analysis Date = 04/18/16 Pct Recovery = 75% Analysis Date = 04/18/16 Pct Recovery = 75% Analysis Date = 04/13/16 Pct Recovery = 75% Analysis Date = 04/13/16 Pct Recovery = 75% Analysis Date = 04/08/16 Pct Recovery = 75% Analysis Date = 04/08/16 Pct Recovery = 75% Analysis Date = 04/03/16 Pct Recovery = 75% Analysis Date = 04/03/16 Pct Recovery = 75% Analysis Date = 03/29/16 Pct Recovery = 75% Analysis Date = 03/29/16 Pct Recovery = 75% Analysis Date = 03/24/16 Pct Recovery = 75% Analysis Date = 03/24/16 Pct Recovery = 75% Analysis Date = 03/19/16 Pct Recovery = 75% Analysis Date = 03/19/16 Pct Recovery = 75% Analysis Date = 03/14/16 Pct Recovery = 75% Analysis Date = 03/14/16 Pct Recovery = 75% Analysis Date = 03/09/16 Pct Recovery = 76% Analysis Date = 03/09/16 Pct Recovery = 76% Analysis Date = 03/04/16 Pct Recovery = 76% Analysis Date = 03/04/16 Pct Recovery = 76% Analysis Date = 02/28/16 Pct Recovery = 76% Analysis Date = 02/28/16 Pct Recovery = 76% Analysis Date = 02/23/16 Pct Recovery = 76% Analysis Date = 02/23/16 Pct Recovery = 76% Analysis Date = 02/18/16 Pct Recovery = 76% Analysis Date = 02/18/16 Pct Recovery = 76% Analysis Date = 02/13/16 Pct Recovery = 76% Analysis Date = 02/13/16 Pct Recovery = 76% Analysis Date = 02/08/16 Pct Recovery = 76% Analysis Date = 02/08/16 Pct Recovery = 76% Analysis Date = 02/03/16 Pct Recovery = 76% Analysis Date = 02/03/16 Pct Recovery = 76% Analysis Date = 01/29/16 Pct Recovery = 76% Analysis Date = 01/29/16 Pct Recovery = 76% Analysis Date = 01/24/16 Pct Recovery = 76% Analysis Date = 01/24/16 Pct Recovery = 76% Analysis Date = 01/19/16 Pct Recovery = 76% Analysis Date = 01/19/16 Pct Recovery = 76% Analysis Date = 01/14/16 Pct Recovery = 76% Analysis Date = 01/14/16 Pct Recovery = 76% Analysis Date = 01/09/16 Pct Recovery = 76% Analysis Date = 01/09/16 Pct Recovery = 76% Analysis Date = 01/04/16 Pct Recovery = 77% Analysis Date = 01/04/16 Pct Recovery = 77% Analysis Date = 12/30/15 Pct Recovery = 77% Analysis Date = 12/30/15 Pct Recovery = 77% Analysis Date = 12/25/15 Pct Recovery = 77% Analysis Date = 12/25/15 Pct Recovery = 77% Analysis Date = 12/20/15 Pct Recovery = 77% Analysis Date = 12/20/15 Pct Recovery = 77% Analysis Date = 12/15/15 Pct Recovery = 77% Analysis Date = 12/15/15 Pct Recovery = 77% Analysis Date = 12/10/15 Pct Recovery = 77% Analysis Date = 12/10/15 Pct Recovery = 77% Analysis Date = 12/05/15 Pct Recovery = 78% Analysis Date = 12/05/15 Pct Recovery = 78% Analysis Date = 11/30/15 Pct Recovery = 78% Analysis Date = 11/30/15 Pct Recovery = 78% Analysis Date = 11/25/15 Pct Recovery = 78% Analysis Date = 11/25/15 Pct Recovery = 78% Analysis Date = 11/20/15 Pct Recovery = 78% Analysis Date = 11/20/15 Pct Recovery = 78% Analysis Date = 11/15/15 Pct Recovery = 78% Analysis Date = 11/15/15 Pct Recovery = 78% Analysis Date = 11/10/15 Pct Recovery = 78% Analysis Date = 11/10/15 Pct Recovery = 78% Analysis Date = 11/05/15 Pct Recovery = 79% Analysis Date = 11/05/15 Pct Recovery = 79% Analysis Date = 10/31/15 Pct Recovery = 79% Analysis Date = 10/31/15 Pct Recovery = 79% Analysis Date = 10/26/15 Pct Recovery = 79% Analysis Date = 10/26/15 Pct Recovery = 79% Analysis Date = 10/21/15 Pct Recovery = 79% Analysis Date = 10/21/15 Pct Recovery = 79% Analysis Date = 10/16/15 Pct Recovery = 79% Analysis Date = 10/16/15 Pct Recovery = 79% Analysis Date = 10/11/15 Pct Recovery = 79% Analysis Date = 10/11/15 Pct Recovery = 79% Analysis Date = 10/06/15 Pct Recovery = 79% Analysis Date = 10/06/15 Pct Recovery = 79% Analysis Date = 10/01/15 Pct Recovery = 79% Analysis Date = 10/01/15 Pct Recovery = 79% Analysis Date = 09/26/15 Pct Recovery = 79% Analysis Date = 09/26/15 Pct Recovery = 79% Analysis Date = 09/21/15 Pct Recovery = 80% Analysis Date = 09/21/15 Pct Recovery = 80% Analysis Date = 09/16/15 Pct Recovery = 80% Analysis Date = 09/16/15 Pct Recovery = 80% Analysis Date = 09/11/15 Pct Recovery = 80% Analysis Date = 09/11/15 Pct Recovery = 80% Analysis Date = 09/05/15 Pct Recovery = 80% Analysis Date = 09/05/15 Pct Recovery = 80% Analysis Date = 08/31/15 Pct Recovery = 80% Analysis Date = 08/31/15 Pct Recovery = 80% Analysis Date = 08/26/15 Pct Recovery = 80% Analysis Date = 08/26/15 Pct Recovery = 80% Analysis Date = 08/21/15 Pct Recovery = 80% Analysis Date = 08/21/15 Pct Recovery = 80% Analysis Date = 08/16/15 Pct Recovery = 80% Analysis Date = 08/16/15 Pct Recovery = 80% Analysis Date = 08/11/15 Pct Recovery = 80% Analysis Date = 08/11/15 Pct Recovery = 80% Analysis Date = 08/06/15 Pct Recovery = 81% Analysis Date = 08/06/15 Pct Recovery = 81% Analysis Date = 08/01/15 Pct Recovery = 81% Analysis Date = 08/01/15 Pct Recovery = 81% Analysis Date = 07/27/15 Pct Recovery = 81% Analysis Date = 07/27/15 Pct Recovery = 81% Analysis Date = 07/22/15 Pct Recovery = 81% Analysis Date = 07/22/15 Pct Recovery = 81% Analysis Date = 07/17/15 Pct Recovery = 81% Analysis Date = 07/17/15 Pct Recovery = 81% Analysis Date = 07/12/15 Pct Recovery = 81% Analysis Date = 07/12/15 Pct Recovery = 81% Analysis Date = 07/07/15 Pct Recovery = 81% Analysis Date = 07/07/15 Pct Recovery = 81% Analysis Date = 07/02/15 Pct Recovery = 81% Analysis Date = 07/02/15 Pct Recovery = 81% Analysis Date = 06/27/15 Pct Recovery = 81% Analysis Date = 06/27/15 Pct Recovery = 81% Analysis Date = 06/22/15 Pct Recovery = 81% Analysis Date = 06/22/15 Pct Recovery = 81% Analysis Date = 06/17/15 Pct Recovery = 80% Analysis Date = 06/17/15 Pct Recovery = 80% Analysis Date = 06/12/15 Pct Recovery = 80% Analysis Date = 06/12/15 Pct Recovery = 80% Analysis Date = 06/07/15 Pct Recovery = 80% Analysis Date = 06/07/15 Pct Recovery = 80% Analysis Date = 06/02/15 Pct Recovery = 80% Analysis Date = 06/02/15 Pct Recovery = 80% Analysis Date = 05/28/15 Pct Recovery = 80% Analysis Date = 05/28/15 Pct Recovery = 80% Analysis Date = 05/23/15 Pct Recovery = 80% Analysis Date = 05/23/15 Pct Recovery = 80% Analysis Date = 05/18/15 Pct Recovery = 80% Analysis Date = 05/18/15 Pct Recovery = 80% Analysis Date = 05/13/15 Pct Recovery = 80% Analysis Date = 05/13/15 Pct Recovery = 80% Analysis Date = 05/08/15 Pct Recovery = 80% Analysis Date = 05/08/15 Pct Recovery = 80% Analysis Date = 05/03/15 Pct Recovery = 80% Analysis Date = 05/03/15 Pct Recovery = 80% Analysis Date = 04/28/15 Pct Recovery = 80% Analysis Date = 04/28/15 Pct Recovery = 80% Analysis Date = 04/23/15 Pct Recovery = 80% Analysis Date = 04/23/15 Pct Recovery = 80% Analysis Date = 04/18/15 Pct Recovery = 80% Analysis Date = 04/18/15 Pct Recovery = 80% Analysis Date = 04/13/15 Pct Recovery = 80% Analysis Date = 04/13/15 Pct Recovery = 80% Analysis Date = 04/08/15 Pct Recovery = 80% Analysis Date = 04/08/15 Pct Recovery = 80% Analysis Date = 04/03/15 Pct Recovery = 80% Analysis Date = 04/03/15 Pct Recovery = 80% Analysis Date = 03/29/15 Pct Recovery = 80% Analysis Date = 03/29/15 Pct Recovery = 80% Analysis Date = 03/24/15 Pct Recovery = 80% Analysis Date = 03/24/15 Pct Recovery = 80% Analysis Date = 03/19/15 Pct Recovery = 80% Analysis Date = 03/19/15 Pct Recovery = 80% Analysis Date = 03/14/15 Pct Recovery = 80% Analysis Date = 03/14/15 Pct Recovery = 80% Analysis Date = 03/09/15 Pct Recovery = 80% Analysis Date = 03/09/15 Pct Recovery = 80% Analysis Date = 03/04/15 Pct Recovery = 80% Analysis Date = 03/04/15 Pct Recovery = 80% Analysis Date = 02/27/15 Pct Recovery = 80% Analysis Date = 02/27/15 Pct Recovery = 80% Analysis Date = 02/22/15 Pct Recovery = 80% Analysis Date = 02/22/15 Pct Recovery = 80% Analysis Date = 02/17/15 Pct Recovery = 80% Analysis Date = 02/17/15 Pct Recovery = 80% Analysis Date = 02/12/15 Pct Recovery = 80% Analysis Date = 02/12/15 Pct Recovery = 80% Analysis Date = 02/07/15 Pct Recovery = 80% Analysis Date = 02/07/15 Pct Recovery = 80% Analysis Date = 02/02/15 Pct Recovery = 80% Analysis Date = 02/02/15 Pct Recovery = 80% Analysis Date = 01/28/15 Pct Recovery = 80% Analysis Date = 01/28/15 Pct Recovery = 80% Analysis Date = 01/23/15 Pct Recovery = 80% Analysis Date = 01/23/15 Pct Recovery = 80% Analysis Date = 01/18/15 Pct Recovery = 80% Analysis Date = 01/18/15 Pct Recovery = 80% Analysis Date = 01/13/15 Pct Recovery = 80% Analysis Date = 01/13/15 Pct Recovery = 80% Analysis Date = 01/08/15 Pct Recovery = 80% Analysis Date = 01/08/15 Pct Recovery = 80% Analysis Date = 01/03/15 Pct Recovery = 80% Analysis Date = 01/03/15 Pct Recovery = 80% Analysis Date = 12/29/14 Pct Recovery = 80% Analysis Date = 12/29/14 Pct Recovery = 80% Analysis Date = 12/24/14 Pct Recovery = 80% Analysis Date = 12/24/14 Pct Recovery = 80% Analysis Date = 12/19/14 Pct Recovery = 80% Analysis Date = 12/19/14 Pct Recovery = 80% Analysis Date = 12/14/14 Pct Recovery = 80% Analysis Date = 12/14/14 Pct Recovery = 80% Analysis Date = 12/09/14 Pct Recovery = 80% Analysis Date = 12/09/14 Pct Recovery = 80% Analysis Date = 12/04/14 Pct Recovery = 80% Analysis Date = 12/04/14 Pct Recovery = 80% Analysis Date = 11/29/14 Pct Recovery = 80% Analysis Date = 11/29/14 Pct Recovery = 80% Analysis Date = 11/24/14 Pct Recovery = 80% Analysis Date = 11/24/14 Pct Recovery = 80% Analysis Date = 11/19/14 Pct Recovery = 80% Analysis Date = 11/19/14 Pct Recovery = 80% Analysis Date = 11/14/14 Pct Recovery = 80% Analysis Date = 11/14/14 Pct Recovery = 80% Analysis Date = 11/09/14 Pct Recovery = 80% Analysis Date = 11/09/14 Pct Recovery = 80% Analysis Date = 11/04/14 Pct Recovery = 80% Analysis Date = 11/04/14 Pct Recovery = 80% Analysis Date = 10/30/14 Pct Recovery = 80% Analysis Date = 10/30/14 Pct Recovery = 80% Analysis Date = 10/25/14 Pct Recovery = 80% Analysis Date = 10/25/14 Pct Recovery = 80% Analysis Date = 10/20/14 Pct Recovery = 80% Analysis Date = 10/20/14 Pct Recovery = 80% Analysis Date = 10/15/14 Pct Recovery = 80% Analysis Date = 10/15/14 Pct Recovery = 80% Analysis Date = 10/10/14 Pct Recovery = 80% Analysis Date = 10/10/14 Pct Recovery = 80% Analysis Date = 10/05/14 Pct Recovery = 80% Analysis Date = 10/05/14 Pct Recovery = 80% Analysis Date = 09/30/14 Pct Recovery = 80% Analysis Date = 09/30/14 Pct Recovery = 80% Analysis Date = 09/25/14 Pct Recovery = 80% Analysis Date = 09/25/14 Pct Recovery = 80% Analysis Date = 09/20/14 Pct Recovery = 80% Analysis Date = 09/20/14 Pct Recovery = 80% Analysis Date = 09/15/14 Pct Recovery = 80% Analysis Date = 09/15/14 Pct Recovery = 80% Analysis Date = 09/10/14 Pct Recovery = 80% Analysis Date = 09/10/14 Pct Recovery = 80% Analysis Date = 09/05/14 Pct Recovery = 80% Analysis Date = 09/05/14 Pct Recovery = 80% Analysis Date = 08/31/14 Pct Recovery = 80% Analysis Date = 08/31/14 Pct Recovery = 80% Analysis Date = 08/26/14 Pct Recovery = 80% Analysis Date = 08/26/14 Pct Recovery = 80% Analysis Date = 08/21/14 Pct Recovery = 80% Analysis Date = 08/21/14 Pct Recovery = 80% Analysis Date = 08/16/14 Pct Recovery = 79% Analysis Date = 08/16/14 Pct Recovery = 79% Analysis Date = 08/11/14 Pct Recovery = 79% Analysis Date = 08/11/14 Pct Recovery = 79% Analysis Date = 08/06/14 Pct Recovery = 79% Analysis Date = 08/06/14 Pct Recovery = 79% Analysis Date = 08/01/14 Pct Recovery = 79% Analysis Date = 08/01/14 Pct Recovery = 79% Analysis Date = 07/27/14 Pct Recovery = 79% Analysis Date = 07/27/14 Pct Recovery = 79% Analysis Date = 07/22/14 Pct Recovery = 79% Analysis Date = 07/22/14 Pct Recovery = 79% Analysis Date = 07/17/14 Pct Recovery = 79% Analysis Date = 07/17/14 Pct Recovery = 79% Analysis Date = 07/12/14 Pct Recovery = 79% Analysis Date = 07/12/14 Pct Recovery = 79% Analysis Date = 07/07/14 Pct Recovery = 79% Analysis Date = 07/07/14 Pct Recovery = 79% Analysis Date = 07/02/14 Pct Recovery = 79% Analysis Date = 07/02/14 Pct Recovery = 79% Analysis Date = 06/27/14 Pct Recovery = 79% Analysis Date = 06/27/14 Pct Recovery = 79% Analysis Date = 06/22/14 Pct Recovery = 79% Analysis Date = 06/22/14 Pct Recovery = 79% Analysis Date = 06/17/14 Pct Recovery = 79% Analysis Date = 06/17/14 Pct Recovery = 79% Analysis Date = 06/12/14 Pct Recovery = 79% Analysis Date = 06/12/14 Pct Recovery = 79% Analysis Date = 06/07/14 Pct Recovery = 79% Analysis Date = 06/07/14 Pct Recovery = 79% Analysis Date = 06/02/14 Pct Recovery = 79% Analysis Date = 06/02/14 Pct Recovery = 79% Analysis Date = 05/28/14 Pct Recovery = 79% Analysis Date = 05/28/14 Pct Recovery = 79% Analysis Date = 05/23/14 Pct Recovery = 79% Analysis Date = 05/23/14 Pct Recovery = 79% Analysis Date = 05/18/14 Pct Recovery = 79% Analysis Date = 05/18/14 Pct Recovery = 79% Analysis Date = 05/13/14 Pct Recovery = 79% Analysis Date = 05/13/14 Pct Recovery = 79% Analysis Date = 05/08/14 Pct Recovery = 79% Analysis Date = 05/08/14 Pct Recovery = 79% Analysis Date = 05/03/14 Pct Recovery = 79% Analysis Date = 05/03/14 Pct Recovery = 79% Analysis Date = 04/28/14 Pct Recovery = 79% Analysis Date = 04/28/14 Pct Recovery = 79% Analysis Date = 04/23/14 Pct Recovery = 79% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
ANTIPYRENE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 2 68% 18% 68% 19%
>= Reporting Level 74 80% 11% 79% 10%
Total 76 79% 12% 79% 10%

Sample Statistics
ANTIPYRENE

Characteristic N % % Basis
Plotted 76 100% Spiked
Estimated Values 5 7% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 76 .  
False Negatives 0 0% 0 out of 76
Not Spiked 39 .  
False Positives 0 0% 0 out of 39

BQS OBSP Determination:
ATENOLOL
METHOD: 2440 , TESTIDCODE: 67502LCM56
Open Data Set

Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 83% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 80% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 63% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 74% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 80 µl & ERA 0406-15-08: 80 µl Pct Recovery = 78% Analysis Date = 11/04/15 SpikeMix = Abs 052215: 80 µl & Abs 050115: 80 µl Pct Recovery = 77% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 69% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 72% Analysis Date = 09/24/16 SpikeMix = Crescent EN160610015: 80 µl & Abs 061416: 80 µl Pct Recovery = 81% Analysis Date = 09/24/16 SpikeMix = Abs 061416: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 76% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 68% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 75% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 83% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 77% Analysis Date = 04/29/15 SpikeMix = ERA 0319-14-05: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 88% Analysis Date = 03/11/15 SpikeMix = ERA 0318-14-02: 15 µl & Abs 041714: 15 µl Pct Recovery = 87% Analysis Date = 02/06/15 SpikeMix = Abs 041814: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 75% Analysis Date = 12/06/14 SpikeMix = ERA 0318-14-02: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 57% Analysis Date = 10/11/14 SpikeMix = ERA 0318-14-02: 60 µl & ERA 0319-14-04: 60 µl Pct Recovery = 70% Analysis Date = 08/21/14 SpikeMix = ERA 0318-14-02: 60 µl & Abs 041714: 60 µl Pct Recovery = 62% Analysis Date = 07/26/14 SpikeMix = ERA 0319-14-05: 60 µl & ERA 0318-14-02: 60 µl Pct Recovery = 82% Analysis Date = 12/07/14 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 65% Analysis Date = 10/25/14 SpikeMix = Abs 041614: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 71% Analysis Date = 06/22/14 SpikeMix = Abs 041814: 60 µl & Abs 041614: 60 µl Pct Recovery = 111% Analysis Date = 06/11/14 SpikeMix = Abs 041614: 60 µl & Abs 041714: 60 µl Pct Recovery = 81% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 80% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 68% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 80% Analysis Date = 02/23/16 SpikeMix = Abs 052215: 40 µl & Abs 050115: 40 µl Pct Recovery = 54% Analysis Date = 07/31/15 SpikeMix = ERA 0406-15-09: 40 µl & Abs 050115: 40 µl Pct Recovery = 98% Analysis Date = 07/30/15 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 75% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-07A: 40 µl & Abs 051315: 40 µl Pct Recovery = 67% Analysis Date = 11/04/15 SpikeMix = ERA 0406-15-07A: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 81% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 65% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 61% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 68% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 83% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 68% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 68% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 65% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 65% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 64% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 60% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 16% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 3% Analysis Date = 12/07/14 SpikeMix = ERA 0318-14-02: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 80% Analysis Date = 11/04/14 SpikeMix = Abs 041814: 8 µl & ERA 0318-14-02: 8 µl Pct Recovery = 80% Analysis Date = 02/10/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 83% Analysis Date = 10/24/14 SpikeMix = ERA 0319-14-05: 8 µl & Abs 041614: 8 µl Pct Recovery = 67% Analysis Date = 10/10/14 SpikeMix = Abs 041814: 30 µl & ERA 0318-14-02: 30 µl Pct Recovery = 59% Analysis Date = 08/30/14 SpikeMix = ERA 0318-14-02: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 78% Analysis Date = 07/20/14 SpikeMix = ERA 0318-14-02: 30 µl & Abs 041714: 30 µl Pct Recovery = 65% Analysis Date = 09/12/14 SpikeMix = Abs 041614: 30 µl & ERA 0319-14-04: 30 µl Pct Recovery = 52% Analysis Date = 07/13/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 74% Analysis Date = 06/28/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 54% Analysis Date = 05/30/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 79% Analysis Date = 05/17/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 83% Analysis Date = 11/25/15 SpikeMix = Abs 050115: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 85% Analysis Date = 11/24/15 SpikeMix = ERA 0406-15-09: 20 µl & Abs 050115: 20 µl Pct Recovery = 74% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 48% Analysis Date = 04/27/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 110% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 51% Analysis Date = 11/24/15 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 96% Analysis Date = 01/18/17 Pct Recovery = 69% Analysis Date = 01/14/17 Pct Recovery = 69% Analysis Date = 01/14/17 Pct Recovery = 69% Analysis Date = 01/09/17 Pct Recovery = 69% Analysis Date = 01/09/17 Pct Recovery = 69% Analysis Date = 01/04/17 Pct Recovery = 69% Analysis Date = 01/04/17 Pct Recovery = 69% Analysis Date = 12/30/16 Pct Recovery = 69% Analysis Date = 12/30/16 Pct Recovery = 69% Analysis Date = 12/25/16 Pct Recovery = 69% Analysis Date = 12/25/16 Pct Recovery = 69% Analysis Date = 12/20/16 Pct Recovery = 68% Analysis Date = 12/20/16 Pct Recovery = 68% Analysis Date = 12/15/16 Pct Recovery = 68% Analysis Date = 12/15/16 Pct Recovery = 68% Analysis Date = 12/10/16 Pct Recovery = 68% Analysis Date = 12/10/16 Pct Recovery = 68% Analysis Date = 12/05/16 Pct Recovery = 68% Analysis Date = 12/05/16 Pct Recovery = 68% Analysis Date = 12/01/16 Pct Recovery = 68% Analysis Date = 12/01/16 Pct Recovery = 68% Analysis Date = 11/26/16 Pct Recovery = 68% Analysis Date = 11/26/16 Pct Recovery = 68% Analysis Date = 11/21/16 Pct Recovery = 68% Analysis Date = 11/21/16 Pct Recovery = 68% Analysis Date = 11/16/16 Pct Recovery = 68% Analysis Date = 11/16/16 Pct Recovery = 68% Analysis Date = 11/11/16 Pct Recovery = 68% Analysis Date = 11/11/16 Pct Recovery = 68% Analysis Date = 11/06/16 Pct Recovery = 68% Analysis Date = 11/06/16 Pct Recovery = 68% Analysis Date = 11/01/16 Pct Recovery = 68% Analysis Date = 11/01/16 Pct Recovery = 68% Analysis Date = 10/27/16 Pct Recovery = 68% Analysis Date = 10/27/16 Pct Recovery = 68% Analysis Date = 10/22/16 Pct Recovery = 67% Analysis Date = 10/22/16 Pct Recovery = 67% Analysis Date = 10/18/16 Pct Recovery = 67% Analysis Date = 10/18/16 Pct Recovery = 67% Analysis Date = 10/13/16 Pct Recovery = 67% Analysis Date = 10/13/16 Pct Recovery = 67% Analysis Date = 10/08/16 Pct Recovery = 67% Analysis Date = 10/08/16 Pct Recovery = 67% Analysis Date = 10/03/16 Pct Recovery = 67% Analysis Date = 10/03/16 Pct Recovery = 67% Analysis Date = 09/28/16 Pct Recovery = 67% Analysis Date = 09/28/16 Pct Recovery = 67% Analysis Date = 09/23/16 Pct Recovery = 67% Analysis Date = 09/23/16 Pct Recovery = 67% Analysis Date = 09/18/16 Pct Recovery = 67% Analysis Date = 09/18/16 Pct Recovery = 67% Analysis Date = 09/13/16 Pct Recovery = 67% Analysis Date = 09/13/16 Pct Recovery = 67% Analysis Date = 09/08/16 Pct Recovery = 67% Analysis Date = 09/08/16 Pct Recovery = 67% Analysis Date = 09/04/16 Pct Recovery = 67% Analysis Date = 09/04/16 Pct Recovery = 67% Analysis Date = 08/30/16 Pct Recovery = 67% Analysis Date = 08/30/16 Pct Recovery = 67% Analysis Date = 08/25/16 Pct Recovery = 67% Analysis Date = 08/25/16 Pct Recovery = 67% Analysis Date = 08/20/16 Pct Recovery = 67% Analysis Date = 08/20/16 Pct Recovery = 67% Analysis Date = 08/15/16 Pct Recovery = 67% Analysis Date = 08/15/16 Pct Recovery = 67% Analysis Date = 08/10/16 Pct Recovery = 67% Analysis Date = 08/10/16 Pct Recovery = 67% Analysis Date = 08/05/16 Pct Recovery = 67% Analysis Date = 08/05/16 Pct Recovery = 67% Analysis Date = 07/31/16 Pct Recovery = 67% Analysis Date = 07/31/16 Pct Recovery = 67% Analysis Date = 07/26/16 Pct Recovery = 67% Analysis Date = 07/26/16 Pct Recovery = 67% Analysis Date = 07/22/16 Pct Recovery = 67% Analysis Date = 07/22/16 Pct Recovery = 67% Analysis Date = 07/17/16 Pct Recovery = 67% Analysis Date = 07/17/16 Pct Recovery = 67% Analysis Date = 07/12/16 Pct Recovery = 67% Analysis Date = 07/12/16 Pct Recovery = 67% Analysis Date = 07/07/16 Pct Recovery = 67% Analysis Date = 07/07/16 Pct Recovery = 67% Analysis Date = 07/02/16 Pct Recovery = 68% Analysis Date = 07/02/16 Pct Recovery = 68% Analysis Date = 06/27/16 Pct Recovery = 68% Analysis Date = 06/27/16 Pct Recovery = 68% Analysis Date = 06/22/16 Pct Recovery = 68% Analysis Date = 06/22/16 Pct Recovery = 68% Analysis Date = 06/17/16 Pct Recovery = 68% Analysis Date = 06/17/16 Pct Recovery = 68% Analysis Date = 06/12/16 Pct Recovery = 68% Analysis Date = 06/12/16 Pct Recovery = 68% Analysis Date = 06/08/16 Pct Recovery = 68% Analysis Date = 06/08/16 Pct Recovery = 68% Analysis Date = 06/03/16 Pct Recovery = 68% Analysis Date = 06/03/16 Pct Recovery = 68% Analysis Date = 05/29/16 Pct Recovery = 69% Analysis Date = 05/29/16 Pct Recovery = 69% Analysis Date = 05/24/16 Pct Recovery = 69% Analysis Date = 05/24/16 Pct Recovery = 69% Analysis Date = 05/19/16 Pct Recovery = 69% Analysis Date = 05/19/16 Pct Recovery = 69% Analysis Date = 05/14/16 Pct Recovery = 69% Analysis Date = 05/14/16 Pct Recovery = 69% Analysis Date = 05/09/16 Pct Recovery = 69% Analysis Date = 05/09/16 Pct Recovery = 69% Analysis Date = 05/04/16 Pct Recovery = 69% Analysis Date = 05/04/16 Pct Recovery = 69% Analysis Date = 04/29/16 Pct Recovery = 70% Analysis Date = 04/29/16 Pct Recovery = 70% Analysis Date = 04/25/16 Pct Recovery = 70% Analysis Date = 04/25/16 Pct Recovery = 70% Analysis Date = 04/20/16 Pct Recovery = 70% Analysis Date = 04/20/16 Pct Recovery = 70% Analysis Date = 04/15/16 Pct Recovery = 70% Analysis Date = 04/15/16 Pct Recovery = 70% Analysis Date = 04/10/16 Pct Recovery = 71% Analysis Date = 04/10/16 Pct Recovery = 71% Analysis Date = 04/05/16 Pct Recovery = 71% Analysis Date = 04/05/16 Pct Recovery = 71% Analysis Date = 03/31/16 Pct Recovery = 71% Analysis Date = 03/31/16 Pct Recovery = 71% Analysis Date = 03/26/16 Pct Recovery = 71% Analysis Date = 03/26/16 Pct Recovery = 71% Analysis Date = 03/21/16 Pct Recovery = 72% Analysis Date = 03/21/16 Pct Recovery = 72% Analysis Date = 03/16/16 Pct Recovery = 72% Analysis Date = 03/16/16 Pct Recovery = 72% Analysis Date = 03/12/16 Pct Recovery = 72% Analysis Date = 03/12/16 Pct Recovery = 72% Analysis Date = 03/07/16 Pct Recovery = 73% Analysis Date = 03/07/16 Pct Recovery = 73% Analysis Date = 03/02/16 Pct Recovery = 73% Analysis Date = 03/02/16 Pct Recovery = 73% Analysis Date = 02/26/16 Pct Recovery = 73% Analysis Date = 02/26/16 Pct Recovery = 73% Analysis Date = 02/21/16 Pct Recovery = 73% Analysis Date = 02/21/16 Pct Recovery = 73% Analysis Date = 02/16/16 Pct Recovery = 74% Analysis Date = 02/16/16 Pct Recovery = 74% Analysis Date = 02/11/16 Pct Recovery = 74% Analysis Date = 02/11/16 Pct Recovery = 74% Analysis Date = 02/06/16 Pct Recovery = 74% Analysis Date = 02/06/16 Pct Recovery = 74% Analysis Date = 02/01/16 Pct Recovery = 74% Analysis Date = 02/01/16 Pct Recovery = 74% Analysis Date = 01/28/16 Pct Recovery = 75% Analysis Date = 01/28/16 Pct Recovery = 75% Analysis Date = 01/23/16 Pct Recovery = 75% Analysis Date = 01/23/16 Pct Recovery = 75% Analysis Date = 01/18/16 Pct Recovery = 75% Analysis Date = 01/18/16 Pct Recovery = 75% Analysis Date = 01/13/16 Pct Recovery = 76% Analysis Date = 01/13/16 Pct Recovery = 76% Analysis Date = 01/08/16 Pct Recovery = 76% Analysis Date = 01/08/16 Pct Recovery = 76% Analysis Date = 01/03/16 Pct Recovery = 76% Analysis Date = 01/03/16 Pct Recovery = 76% Analysis Date = 12/29/15 Pct Recovery = 76% Analysis Date = 12/29/15 Pct Recovery = 76% Analysis Date = 12/24/15 Pct Recovery = 77% Analysis Date = 12/24/15 Pct Recovery = 77% Analysis Date = 12/19/15 Pct Recovery = 77% Analysis Date = 12/19/15 Pct Recovery = 77% Analysis Date = 12/15/15 Pct Recovery = 77% Analysis Date = 12/15/15 Pct Recovery = 77% Analysis Date = 12/10/15 Pct Recovery = 77% Analysis Date = 12/10/15 Pct Recovery = 77% Analysis Date = 12/05/15 Pct Recovery = 78% Analysis Date = 12/05/15 Pct Recovery = 78% Analysis Date = 11/30/15 Pct Recovery = 78% Analysis Date = 11/30/15 Pct Recovery = 78% Analysis Date = 11/25/15 Pct Recovery = 78% Analysis Date = 11/25/15 Pct Recovery = 78% Analysis Date = 11/20/15 Pct Recovery = 78% Analysis Date = 11/20/15 Pct Recovery = 78% Analysis Date = 11/15/15 Pct Recovery = 78% Analysis Date = 11/15/15 Pct Recovery = 78% Analysis Date = 11/10/15 Pct Recovery = 78% Analysis Date = 11/10/15 Pct Recovery = 78% Analysis Date = 11/05/15 Pct Recovery = 78% Analysis Date = 11/05/15 Pct Recovery = 78% Analysis Date = 11/01/15 Pct Recovery = 78% Analysis Date = 11/01/15 Pct Recovery = 78% Analysis Date = 10/27/15 Pct Recovery = 78% Analysis Date = 10/27/15 Pct Recovery = 78% Analysis Date = 10/22/15 Pct Recovery = 78% Analysis Date = 10/22/15 Pct Recovery = 78% Analysis Date = 10/17/15 Pct Recovery = 78% Analysis Date = 10/17/15 Pct Recovery = 78% Analysis Date = 10/12/15 Pct Recovery = 78% Analysis Date = 10/12/15 Pct Recovery = 78% Analysis Date = 10/07/15 Pct Recovery = 78% Analysis Date = 10/07/15 Pct Recovery = 78% Analysis Date = 10/02/15 Pct Recovery = 78% Analysis Date = 10/02/15 Pct Recovery = 78% Analysis Date = 09/27/15 Pct Recovery = 78% Analysis Date = 09/27/15 Pct Recovery = 78% Analysis Date = 09/22/15 Pct Recovery = 78% Analysis Date = 09/22/15 Pct Recovery = 78% Analysis Date = 09/17/15 Pct Recovery = 78% Analysis Date = 09/17/15 Pct Recovery = 78% Analysis Date = 09/13/15 Pct Recovery = 78% Analysis Date = 09/13/15 Pct Recovery = 78% Analysis Date = 09/08/15 Pct Recovery = 78% Analysis Date = 09/08/15 Pct Recovery = 78% Analysis Date = 09/03/15 Pct Recovery = 78% Analysis Date = 09/03/15 Pct Recovery = 78% Analysis Date = 08/29/15 Pct Recovery = 78% Analysis Date = 08/29/15 Pct Recovery = 78% Analysis Date = 08/24/15 Pct Recovery = 78% Analysis Date = 08/24/15 Pct Recovery = 78% Analysis Date = 08/19/15 Pct Recovery = 78% Analysis Date = 08/19/15 Pct Recovery = 78% Analysis Date = 08/14/15 Pct Recovery = 78% Analysis Date = 08/14/15 Pct Recovery = 78% Analysis Date = 08/09/15 Pct Recovery = 78% Analysis Date = 08/09/15 Pct Recovery = 78% Analysis Date = 08/04/15 Pct Recovery = 78% Analysis Date = 08/04/15 Pct Recovery = 78% Analysis Date = 07/31/15 Pct Recovery = 78% Analysis Date = 07/31/15 Pct Recovery = 78% Analysis Date = 07/26/15 Pct Recovery = 78% Analysis Date = 07/26/15 Pct Recovery = 78% Analysis Date = 07/21/15 Pct Recovery = 78% Analysis Date = 07/21/15 Pct Recovery = 78% Analysis Date = 07/16/15 Pct Recovery = 78% Analysis Date = 07/16/15 Pct Recovery = 78% Analysis Date = 07/11/15 Pct Recovery = 78% Analysis Date = 07/11/15 Pct Recovery = 78% Analysis Date = 07/06/15 Pct Recovery = 78% Analysis Date = 07/06/15 Pct Recovery = 78% Analysis Date = 07/01/15 Pct Recovery = 78% Analysis Date = 07/01/15 Pct Recovery = 78% Analysis Date = 06/26/15 Pct Recovery = 78% Analysis Date = 06/26/15 Pct Recovery = 78% Analysis Date = 06/21/15 Pct Recovery = 78% Analysis Date = 06/21/15 Pct Recovery = 78% Analysis Date = 06/17/15 Pct Recovery = 78% Analysis Date = 06/17/15 Pct Recovery = 78% Analysis Date = 06/12/15 Pct Recovery = 78% Analysis Date = 06/12/15 Pct Recovery = 78% Analysis Date = 06/07/15 Pct Recovery = 78% Analysis Date = 06/07/15 Pct Recovery = 78% Analysis Date = 06/02/15 Pct Recovery = 77% Analysis Date = 06/02/15 Pct Recovery = 77% Analysis Date = 05/28/15 Pct Recovery = 77% Analysis Date = 05/28/15 Pct Recovery = 77% Analysis Date = 05/23/15 Pct Recovery = 77% Analysis Date = 05/23/15 Pct Recovery = 77% Analysis Date = 05/18/15 Pct Recovery = 77% Analysis Date = 05/18/15 Pct Recovery = 77% Analysis Date = 05/13/15 Pct Recovery = 77% Analysis Date = 05/13/15 Pct Recovery = 77% Analysis Date = 05/08/15 Pct Recovery = 77% Analysis Date = 05/08/15 Pct Recovery = 77% Analysis Date = 05/04/15 Pct Recovery = 77% Analysis Date = 05/04/15 Pct Recovery = 77% Analysis Date = 04/29/15 Pct Recovery = 77% Analysis Date = 04/29/15 Pct Recovery = 77% Analysis Date = 04/24/15 Pct Recovery = 77% Analysis Date = 04/24/15 Pct Recovery = 77% Analysis Date = 04/19/15 Pct Recovery = 77% Analysis Date = 04/19/15 Pct Recovery = 77% Analysis Date = 04/14/15 Pct Recovery = 77% Analysis Date = 04/14/15 Pct Recovery = 77% Analysis Date = 04/09/15 Pct Recovery = 77% Analysis Date = 04/09/15 Pct Recovery = 77% Analysis Date = 04/04/15 Pct Recovery = 77% Analysis Date = 04/04/15 Pct Recovery = 77% Analysis Date = 03/30/15 Pct Recovery = 77% Analysis Date = 03/30/15 Pct Recovery = 77% Analysis Date = 03/25/15 Pct Recovery = 77% Analysis Date = 03/25/15 Pct Recovery = 77% Analysis Date = 03/21/15 Pct Recovery = 77% Analysis Date = 03/21/15 Pct Recovery = 77% Analysis Date = 03/16/15 Pct Recovery = 77% Analysis Date = 03/16/15 Pct Recovery = 77% Analysis Date = 03/11/15 Pct Recovery = 76% Analysis Date = 03/11/15 Pct Recovery = 76% Analysis Date = 03/06/15 Pct Recovery = 76% Analysis Date = 03/06/15 Pct Recovery = 76% Analysis Date = 03/01/15 Pct Recovery = 76% Analysis Date = 03/01/15 Pct Recovery = 76% Analysis Date = 02/24/15 Pct Recovery = 76% Analysis Date = 02/24/15 Pct Recovery = 76% Analysis Date = 02/19/15 Pct Recovery = 76% Analysis Date = 02/19/15 Pct Recovery = 76% Analysis Date = 02/14/15 Pct Recovery = 76% Analysis Date = 02/14/15 Pct Recovery = 76% Analysis Date = 02/09/15 Pct Recovery = 76% Analysis Date = 02/09/15 Pct Recovery = 76% Analysis Date = 02/05/15 Pct Recovery = 76% Analysis Date = 02/05/15 Pct Recovery = 76% Analysis Date = 01/31/15 Pct Recovery = 76% Analysis Date = 01/31/15 Pct Recovery = 76% Analysis Date = 01/26/15 Pct Recovery = 76% Analysis Date = 01/26/15 Pct Recovery = 76% Analysis Date = 01/21/15 Pct Recovery = 76% Analysis Date = 01/21/15 Pct Recovery = 76% Analysis Date = 01/16/15 Pct Recovery = 76% Analysis Date = 01/16/15 Pct Recovery = 76% Analysis Date = 01/11/15 Pct Recovery = 76% Analysis Date = 01/11/15 Pct Recovery = 76% Analysis Date = 01/06/15 Pct Recovery = 76% Analysis Date = 01/06/15 Pct Recovery = 76% Analysis Date = 01/01/15 Pct Recovery = 76% Analysis Date = 01/01/15 Pct Recovery = 76% Analysis Date = 12/27/14 Pct Recovery = 75% Analysis Date = 12/27/14 Pct Recovery = 75% Analysis Date = 12/23/14 Pct Recovery = 75% Analysis Date = 12/23/14 Pct Recovery = 75% Analysis Date = 12/18/14 Pct Recovery = 75% Analysis Date = 12/18/14 Pct Recovery = 75% Analysis Date = 12/13/14 Pct Recovery = 75% Analysis Date = 12/13/14 Pct Recovery = 75% Analysis Date = 12/08/14 Pct Recovery = 75% Analysis Date = 12/08/14 Pct Recovery = 75% Analysis Date = 12/03/14 Pct Recovery = 75% Analysis Date = 12/03/14 Pct Recovery = 75% Analysis Date = 11/28/14 Pct Recovery = 75% Analysis Date = 11/28/14 Pct Recovery = 75% Analysis Date = 11/23/14 Pct Recovery = 75% Analysis Date = 11/23/14 Pct Recovery = 75% Analysis Date = 11/18/14 Pct Recovery = 75% Analysis Date = 11/18/14 Pct Recovery = 75% Analysis Date = 11/13/14 Pct Recovery = 75% Analysis Date = 11/13/14 Pct Recovery = 75% Analysis Date = 11/09/14 Pct Recovery = 75% Analysis Date = 11/09/14 Pct Recovery = 75% Analysis Date = 11/04/14 Pct Recovery = 75% Analysis Date = 11/04/14 Pct Recovery = 75% Analysis Date = 10/30/14 Pct Recovery = 75% Analysis Date = 10/30/14 Pct Recovery = 75% Analysis Date = 10/25/14 Pct Recovery = 75% Analysis Date = 10/25/14 Pct Recovery = 75% Analysis Date = 10/20/14 Pct Recovery = 74% Analysis Date = 10/20/14 Pct Recovery = 74% Analysis Date = 10/15/14 Pct Recovery = 74% Analysis Date = 10/15/14 Pct Recovery = 74% Analysis Date = 10/10/14 Pct Recovery = 74% Analysis Date = 10/10/14 Pct Recovery = 74% Analysis Date = 10/05/14 Pct Recovery = 74% Analysis Date = 10/05/14 Pct Recovery = 74% Analysis Date = 09/30/14 Pct Recovery = 74% Analysis Date = 09/30/14 Pct Recovery = 74% Analysis Date = 09/26/14 Pct Recovery = 74% Analysis Date = 09/26/14 Pct Recovery = 74% Analysis Date = 09/21/14 Pct Recovery = 74% Analysis Date = 09/21/14 Pct Recovery = 74% Analysis Date = 09/16/14 Pct Recovery = 74% Analysis Date = 09/16/14 Pct Recovery = 74% Analysis Date = 09/11/14 Pct Recovery = 74% Analysis Date = 09/11/14 Pct Recovery = 74% Analysis Date = 09/06/14 Pct Recovery = 74% Analysis Date = 09/06/14 Pct Recovery = 74% Analysis Date = 09/01/14 Pct Recovery = 74% Analysis Date = 09/01/14 Pct Recovery = 74% Analysis Date = 08/27/14 Pct Recovery = 74% Analysis Date = 08/27/14 Pct Recovery = 74% Analysis Date = 08/22/14 Pct Recovery = 74% Analysis Date = 08/22/14 Pct Recovery = 74% Analysis Date = 08/17/14 Pct Recovery = 74% Analysis Date = 08/17/14 Pct Recovery = 74% Analysis Date = 08/13/14 Pct Recovery = 73% Analysis Date = 08/13/14 Pct Recovery = 73% Analysis Date = 08/08/14 Pct Recovery = 73% Analysis Date = 08/08/14 Pct Recovery = 73% Analysis Date = 08/03/14 Pct Recovery = 73% Analysis Date = 08/03/14 Pct Recovery = 73% Analysis Date = 07/29/14 Pct Recovery = 73% Analysis Date = 07/29/14 Pct Recovery = 73% Analysis Date = 07/24/14 Pct Recovery = 73% Analysis Date = 07/24/14 Pct Recovery = 73% Analysis Date = 07/19/14 Pct Recovery = 73% Analysis Date = 07/19/14 Pct Recovery = 73% Analysis Date = 07/14/14 Pct Recovery = 73% Analysis Date = 07/14/14 Pct Recovery = 73% Analysis Date = 07/09/14 Pct Recovery = 73% Analysis Date = 07/09/14 Pct Recovery = 73% Analysis Date = 07/04/14 Pct Recovery = 73% Analysis Date = 07/04/14 Pct Recovery = 73% Analysis Date = 06/30/14 Pct Recovery = 73% Analysis Date = 06/30/14 Pct Recovery = 73% Analysis Date = 06/25/14 Pct Recovery = 73% Analysis Date = 06/25/14 Pct Recovery = 73% Analysis Date = 06/20/14 Pct Recovery = 73% Analysis Date = 06/20/14 Pct Recovery = 73% Analysis Date = 06/15/14 Pct Recovery = 73% Analysis Date = 06/15/14 Pct Recovery = 73% Analysis Date = 06/10/14 Pct Recovery = 73% Analysis Date = 06/10/14 Pct Recovery = 73% Analysis Date = 06/05/14 Pct Recovery = 73% Analysis Date = 06/05/14 Pct Recovery = 73% Analysis Date = 05/31/14 Pct Recovery = 73% Analysis Date = 05/31/14 Pct Recovery = 73% Analysis Date = 05/26/14 Pct Recovery = 72% Analysis Date = 05/26/14 Pct Recovery = 72% Analysis Date = 05/21/14 Pct Recovery = 72% Analysis Date = 05/21/14 Pct Recovery = 72% Analysis Date = 05/17/14 Pct Recovery = 72% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
ATENOLOL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 63 72% 17% 74% 12%
Total 63 72% 17% 74% 12%

Sample Statistics
ATENOLOL

Characteristic N % % Basis
Plotted 63 81% Spiked
Estimated Values 4 5% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 5 6% Spiked
Spiked 78 .  
False Negatives 10 13% 10 out of 78
Not Spiked 37 .  
False Positives 0 0% 0 out of 37

BQS OBSP Determination:
ATRAZINE
METHOD: 2440 , TESTIDCODE: 65065LCM56
Open Data Set

Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 85% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 87% Analysis Date = 11/24/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 82% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 80 µl & Abs 051315: 80 µl Pct Recovery = 94% Analysis Date = 10/01/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 109% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 80 µl & ERA 0406-15-08: 80 µl Pct Recovery = 83% Analysis Date = 11/05/15 SpikeMix = ERA 0406-15-08: 80 µl & Abs 052215: 80 µl Pct Recovery = 75% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 76% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 78% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 88% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 90% Analysis Date = 11/18/16 SpikeMix = ERA 04281604: 80 µl & ERA 04281603: 80 µl Pct Recovery = 76% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & ERA 04281604: 80 µl Pct Recovery = 74% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 73% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 74% Analysis Date = 05/07/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 99% Analysis Date = 04/29/15 SpikeMix = ERA 0319-14-05: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 87% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 80% Analysis Date = 01/16/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 86% Analysis Date = 12/07/14 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 77% Analysis Date = 12/06/14 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 70% Analysis Date = 08/28/14 SpikeMix = ERA 0319-14-04: 60 µl & ERA 0319-14-05: 60 µl Pct Recovery = 63% Analysis Date = 07/26/14 SpikeMix = ERA 0319-14-05: 60 µl & ERA 0318-14-02: 60 µl Pct Recovery = 88% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-04: 15 µl & Abs 041814: 15 µl Pct Recovery = 77% Analysis Date = 02/06/15 SpikeMix = Abs 041814: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 91% Analysis Date = 07/12/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 76% Analysis Date = 06/22/14 SpikeMix = Abs 041814: 60 µl & Abs 041614: 60 µl Pct Recovery = 92% Analysis Date = 05/21/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 71% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 82% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 70% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-07A: 40 µl & Abs 051315: 40 µl Pct Recovery = 62% Analysis Date = 07/31/15 SpikeMix = Abs 051315: 40 µl & Abs 052215: 40 µl Pct Recovery = 71% Analysis Date = 07/30/15 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 75% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-08: 40 µl & Abs 052215: 40 µl Pct Recovery = 79% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 70% Analysis Date = 11/04/15 SpikeMix = ERA 0406-15-07A: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 71% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-08: 40 µl & ERA 0406-15-09: 40 µl Pct Recovery = 73% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 96% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 98% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 87% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 83% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 104% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 105% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 64% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 69% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 87% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 74% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 75% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 81% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 73% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 74% Analysis Date = 11/04/14 SpikeMix = Abs 041714: 8 µl & ERA 0319-14-05: 8 µl Pct Recovery = 70% Analysis Date = 10/24/14 SpikeMix = ERA 0319-14-05: 8 µl & Abs 041614: 8 µl Pct Recovery = 84% Analysis Date = 04/10/15 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 79% Analysis Date = 11/04/14 SpikeMix = Abs 041814: 8 µl & ERA 0318-14-02: 8 µl Pct Recovery = 85% Analysis Date = 10/11/14 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 60% Analysis Date = 04/23/14 SpikeMix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.2: 20 µl Pct Recovery = 81% Analysis Date = 08/30/14 SpikeMix = ERA 0318-14-02: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 69% Analysis Date = 08/16/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 39% Analysis Date = 07/13/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 67% Analysis Date = 10/10/14 SpikeMix = Abs 041714: 30 µl & Abs 041814: 30 µl Pct Recovery = 79% Analysis Date = 10/10/14 SpikeMix = Abs 041814: 30 µl & ERA 0318-14-02: 30 µl Pct Recovery = 65% Analysis Date = 07/13/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 74% Analysis Date = 05/30/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 94% Analysis Date = 02/23/16 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 76% Analysis Date = 06/26/15 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 74% Analysis Date = 06/09/15 SpikeMix = Abs 051315: 20 µl & Abs 050115: 20 µl Pct Recovery = 72% Analysis Date = 04/27/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 97% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 84% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-08: 20 µl & ERA 0406-15-09: 20 µl Pct Recovery = 50% Analysis Date = 11/25/15 SpikeMix = Abs 050115: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 77% Analysis Date = 09/15/15 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 73% Analysis Date = 09/09/15 SpikeMix = ERA 0406-15-08: 20 µl & Abs 052215: 20 µl Pct Recovery = 87% Analysis Date = 04/09/16 SpikeMix = Abs 051315: 10 µl & ERA 0406-15-09: 10 µl Pct Recovery = 69% Analysis Date = 04/09/16 SpikeMix = Abs 051315: 10 µl & ERA 0406-15-09: 10 µl Pct Recovery = 70% Analysis Date = 01/18/17 Pct Recovery = 85% Analysis Date = 01/13/17 Pct Recovery = 85% Analysis Date = 01/13/17 Pct Recovery = 85% Analysis Date = 01/08/17 Pct Recovery = 85% Analysis Date = 01/08/17 Pct Recovery = 85% Analysis Date = 01/03/17 Pct Recovery = 85% Analysis Date = 01/03/17 Pct Recovery = 85% Analysis Date = 12/29/16 Pct Recovery = 85% Analysis Date = 12/29/16 Pct Recovery = 85% Analysis Date = 12/24/16 Pct Recovery = 85% Analysis Date = 12/24/16 Pct Recovery = 85% Analysis Date = 12/19/16 Pct Recovery = 85% Analysis Date = 12/19/16 Pct Recovery = 85% Analysis Date = 12/14/16 Pct Recovery = 84% Analysis Date = 12/14/16 Pct Recovery = 84% Analysis Date = 12/09/16 Pct Recovery = 84% Analysis Date = 12/09/16 Pct Recovery = 84% Analysis Date = 12/04/16 Pct Recovery = 84% Analysis Date = 12/04/16 Pct Recovery = 84% Analysis Date = 11/29/16 Pct Recovery = 84% Analysis Date = 11/29/16 Pct Recovery = 84% Analysis Date = 11/24/16 Pct Recovery = 84% Analysis Date = 11/24/16 Pct Recovery = 84% Analysis Date = 11/19/16 Pct Recovery = 84% Analysis Date = 11/19/16 Pct Recovery = 84% Analysis Date = 11/14/16 Pct Recovery = 83% Analysis Date = 11/14/16 Pct Recovery = 83% Analysis Date = 11/09/16 Pct Recovery = 83% Analysis Date = 11/09/16 Pct Recovery = 83% Analysis Date = 11/04/16 Pct Recovery = 83% Analysis Date = 11/04/16 Pct Recovery = 83% Analysis Date = 10/30/16 Pct Recovery = 83% Analysis Date = 10/30/16 Pct Recovery = 83% Analysis Date = 10/25/16 Pct Recovery = 83% Analysis Date = 10/25/16 Pct Recovery = 83% Analysis Date = 10/20/16 Pct Recovery = 83% Analysis Date = 10/20/16 Pct Recovery = 83% Analysis Date = 10/15/16 Pct Recovery = 83% Analysis Date = 10/15/16 Pct Recovery = 83% Analysis Date = 10/10/16 Pct Recovery = 82% Analysis Date = 10/10/16 Pct Recovery = 82% Analysis Date = 10/05/16 Pct Recovery = 82% Analysis Date = 10/05/16 Pct Recovery = 82% Analysis Date = 09/30/16 Pct Recovery = 82% Analysis Date = 09/30/16 Pct Recovery = 82% Analysis Date = 09/25/16 Pct Recovery = 82% Analysis Date = 09/25/16 Pct Recovery = 82% Analysis Date = 09/20/16 Pct Recovery = 82% Analysis Date = 09/20/16 Pct Recovery = 82% Analysis Date = 09/15/16 Pct Recovery = 82% Analysis Date = 09/15/16 Pct Recovery = 82% Analysis Date = 09/10/16 Pct Recovery = 81% Analysis Date = 09/10/16 Pct Recovery = 81% Analysis Date = 09/05/16 Pct Recovery = 81% Analysis Date = 09/05/16 Pct Recovery = 81% Analysis Date = 08/31/16 Pct Recovery = 81% Analysis Date = 08/31/16 Pct Recovery = 81% Analysis Date = 08/26/16 Pct Recovery = 81% Analysis Date = 08/26/16 Pct Recovery = 81% Analysis Date = 08/21/16 Pct Recovery = 81% Analysis Date = 08/21/16 Pct Recovery = 81% Analysis Date = 08/16/16 Pct Recovery = 81% Analysis Date = 08/16/16 Pct Recovery = 81% Analysis Date = 08/11/16 Pct Recovery = 81% Analysis Date = 08/11/16 Pct Recovery = 81% Analysis Date = 08/06/16 Pct Recovery = 80% Analysis Date = 08/06/16 Pct Recovery = 80% Analysis Date = 08/01/16 Pct Recovery = 80% Analysis Date = 08/01/16 Pct Recovery = 80% Analysis Date = 07/27/16 Pct Recovery = 80% Analysis Date = 07/27/16 Pct Recovery = 80% Analysis Date = 07/22/16 Pct Recovery = 80% Analysis Date = 07/22/16 Pct Recovery = 80% Analysis Date = 07/17/16 Pct Recovery = 80% Analysis Date = 07/17/16 Pct Recovery = 80% Analysis Date = 07/12/16 Pct Recovery = 80% Analysis Date = 07/12/16 Pct Recovery = 80% Analysis Date = 07/07/16 Pct Recovery = 80% Analysis Date = 07/07/16 Pct Recovery = 80% Analysis Date = 07/02/16 Pct Recovery = 80% Analysis Date = 07/02/16 Pct Recovery = 80% Analysis Date = 06/27/16 Pct Recovery = 80% Analysis Date = 06/27/16 Pct Recovery = 80% Analysis Date = 06/22/16 Pct Recovery = 79% Analysis Date = 06/22/16 Pct Recovery = 79% Analysis Date = 06/17/16 Pct Recovery = 79% Analysis Date = 06/17/16 Pct Recovery = 79% Analysis Date = 06/12/16 Pct Recovery = 79% Analysis Date = 06/12/16 Pct Recovery = 79% Analysis Date = 06/07/16 Pct Recovery = 79% Analysis Date = 06/07/16 Pct Recovery = 79% Analysis Date = 06/02/16 Pct Recovery = 79% Analysis Date = 06/02/16 Pct Recovery = 79% Analysis Date = 05/28/16 Pct Recovery = 79% Analysis Date = 05/28/16 Pct Recovery = 79% Analysis Date = 05/23/16 Pct Recovery = 79% Analysis Date = 05/23/16 Pct Recovery = 79% Analysis Date = 05/18/16 Pct Recovery = 79% Analysis Date = 05/18/16 Pct Recovery = 79% Analysis Date = 05/13/16 Pct Recovery = 79% Analysis Date = 05/13/16 Pct Recovery = 79% Analysis Date = 05/08/16 Pct Recovery = 78% Analysis Date = 05/08/16 Pct Recovery = 78% Analysis Date = 05/03/16 Pct Recovery = 78% Analysis Date = 05/03/16 Pct Recovery = 78% Analysis Date = 04/28/16 Pct Recovery = 78% Analysis Date = 04/28/16 Pct Recovery = 78% Analysis Date = 04/23/16 Pct Recovery = 78% Analysis Date = 04/23/16 Pct Recovery = 78% Analysis Date = 04/18/16 Pct Recovery = 78% Analysis Date = 04/18/16 Pct Recovery = 78% Analysis Date = 04/13/16 Pct Recovery = 78% Analysis Date = 04/13/16 Pct Recovery = 78% Analysis Date = 04/08/16 Pct Recovery = 78% Analysis Date = 04/08/16 Pct Recovery = 78% Analysis Date = 04/03/16 Pct Recovery = 78% Analysis Date = 04/03/16 Pct Recovery = 78% Analysis Date = 03/29/16 Pct Recovery = 78% Analysis Date = 03/29/16 Pct Recovery = 78% Analysis Date = 03/24/16 Pct Recovery = 78% Analysis Date = 03/24/16 Pct Recovery = 78% Analysis Date = 03/19/16 Pct Recovery = 78% Analysis Date = 03/19/16 Pct Recovery = 78% Analysis Date = 03/14/16 Pct Recovery = 78% Analysis Date = 03/14/16 Pct Recovery = 78% Analysis Date = 03/09/16 Pct Recovery = 78% Analysis Date = 03/09/16 Pct Recovery = 78% Analysis Date = 03/04/16 Pct Recovery = 78% Analysis Date = 03/04/16 Pct Recovery = 78% Analysis Date = 02/28/16 Pct Recovery = 78% Analysis Date = 02/28/16 Pct Recovery = 78% Analysis Date = 02/23/16 Pct Recovery = 78% Analysis Date = 02/23/16 Pct Recovery = 78% Analysis Date = 02/18/16 Pct Recovery = 78% Analysis Date = 02/18/16 Pct Recovery = 78% Analysis Date = 02/13/16 Pct Recovery = 78% Analysis Date = 02/13/16 Pct Recovery = 78% Analysis Date = 02/08/16 Pct Recovery = 78% Analysis Date = 02/08/16 Pct Recovery = 78% Analysis Date = 02/03/16 Pct Recovery = 78% Analysis Date = 02/03/16 Pct Recovery = 78% Analysis Date = 01/29/16 Pct Recovery = 78% Analysis Date = 01/29/16 Pct Recovery = 78% Analysis Date = 01/24/16 Pct Recovery = 78% Analysis Date = 01/24/16 Pct Recovery = 78% Analysis Date = 01/19/16 Pct Recovery = 78% Analysis Date = 01/19/16 Pct Recovery = 78% Analysis Date = 01/14/16 Pct Recovery = 78% Analysis Date = 01/14/16 Pct Recovery = 78% Analysis Date = 01/09/16 Pct Recovery = 78% Analysis Date = 01/09/16 Pct Recovery = 78% Analysis Date = 01/04/16 Pct Recovery = 78% Analysis Date = 01/04/16 Pct Recovery = 78% Analysis Date = 12/30/15 Pct Recovery = 78% Analysis Date = 12/30/15 Pct Recovery = 78% Analysis Date = 12/25/15 Pct Recovery = 78% Analysis Date = 12/25/15 Pct Recovery = 78% Analysis Date = 12/20/15 Pct Recovery = 78% Analysis Date = 12/20/15 Pct Recovery = 78% Analysis Date = 12/15/15 Pct Recovery = 78% Analysis Date = 12/15/15 Pct Recovery = 78% Analysis Date = 12/10/15 Pct Recovery = 78% Analysis Date = 12/10/15 Pct Recovery = 78% Analysis Date = 12/05/15 Pct Recovery = 78% Analysis Date = 12/05/15 Pct Recovery = 78% Analysis Date = 11/30/15 Pct Recovery = 78% Analysis Date = 11/30/15 Pct Recovery = 78% Analysis Date = 11/25/15 Pct Recovery = 78% Analysis Date = 11/25/15 Pct Recovery = 78% Analysis Date = 11/20/15 Pct Recovery = 78% Analysis Date = 11/20/15 Pct Recovery = 78% Analysis Date = 11/15/15 Pct Recovery = 78% Analysis Date = 11/15/15 Pct Recovery = 78% Analysis Date = 11/10/15 Pct Recovery = 78% Analysis Date = 11/10/15 Pct Recovery = 78% Analysis Date = 11/05/15 Pct Recovery = 78% Analysis Date = 11/05/15 Pct Recovery = 78% Analysis Date = 10/31/15 Pct Recovery = 78% Analysis Date = 10/31/15 Pct Recovery = 78% Analysis Date = 10/26/15 Pct Recovery = 78% Analysis Date = 10/26/15 Pct Recovery = 78% Analysis Date = 10/21/15 Pct Recovery = 78% Analysis Date = 10/21/15 Pct Recovery = 78% Analysis Date = 10/16/15 Pct Recovery = 78% Analysis Date = 10/16/15 Pct Recovery = 78% Analysis Date = 10/11/15 Pct Recovery = 78% Analysis Date = 10/11/15 Pct Recovery = 78% Analysis Date = 10/06/15 Pct Recovery = 78% Analysis Date = 10/06/15 Pct Recovery = 78% Analysis Date = 10/01/15 Pct Recovery = 78% Analysis Date = 10/01/15 Pct Recovery = 78% Analysis Date = 09/26/15 Pct Recovery = 79% Analysis Date = 09/26/15 Pct Recovery = 79% Analysis Date = 09/21/15 Pct Recovery = 79% Analysis Date = 09/21/15 Pct Recovery = 79% Analysis Date = 09/16/15 Pct Recovery = 79% Analysis Date = 09/16/15 Pct Recovery = 79% Analysis Date = 09/11/15 Pct Recovery = 79% Analysis Date = 09/11/15 Pct Recovery = 79% Analysis Date = 09/05/15 Pct Recovery = 79% Analysis Date = 09/05/15 Pct Recovery = 79% Analysis Date = 08/31/15 Pct Recovery = 79% Analysis Date = 08/31/15 Pct Recovery = 79% Analysis Date = 08/26/15 Pct Recovery = 79% Analysis Date = 08/26/15 Pct Recovery = 79% Analysis Date = 08/21/15 Pct Recovery = 79% Analysis Date = 08/21/15 Pct Recovery = 79% Analysis Date = 08/16/15 Pct Recovery = 79% Analysis Date = 08/16/15 Pct Recovery = 79% Analysis Date = 08/11/15 Pct Recovery = 79% Analysis Date = 08/11/15 Pct Recovery = 79% Analysis Date = 08/06/15 Pct Recovery = 79% Analysis Date = 08/06/15 Pct Recovery = 79% Analysis Date = 08/01/15 Pct Recovery = 79% Analysis Date = 08/01/15 Pct Recovery = 79% Analysis Date = 07/27/15 Pct Recovery = 79% Analysis Date = 07/27/15 Pct Recovery = 79% Analysis Date = 07/22/15 Pct Recovery = 79% Analysis Date = 07/22/15 Pct Recovery = 79% Analysis Date = 07/17/15 Pct Recovery = 79% Analysis Date = 07/17/15 Pct Recovery = 79% Analysis Date = 07/12/15 Pct Recovery = 79% Analysis Date = 07/12/15 Pct Recovery = 79% Analysis Date = 07/07/15 Pct Recovery = 79% Analysis Date = 07/07/15 Pct Recovery = 79% Analysis Date = 07/02/15 Pct Recovery = 79% Analysis Date = 07/02/15 Pct Recovery = 79% Analysis Date = 06/27/15 Pct Recovery = 79% Analysis Date = 06/27/15 Pct Recovery = 79% Analysis Date = 06/22/15 Pct Recovery = 79% Analysis Date = 06/22/15 Pct Recovery = 79% Analysis Date = 06/17/15 Pct Recovery = 79% Analysis Date = 06/17/15 Pct Recovery = 79% Analysis Date = 06/12/15 Pct Recovery = 79% Analysis Date = 06/12/15 Pct Recovery = 79% Analysis Date = 06/07/15 Pct Recovery = 79% Analysis Date = 06/07/15 Pct Recovery = 79% Analysis Date = 06/02/15 Pct Recovery = 79% Analysis Date = 06/02/15 Pct Recovery = 79% Analysis Date = 05/28/15 Pct Recovery = 79% Analysis Date = 05/28/15 Pct Recovery = 79% Analysis Date = 05/23/15 Pct Recovery = 79% Analysis Date = 05/23/15 Pct Recovery = 79% Analysis Date = 05/18/15 Pct Recovery = 79% Analysis Date = 05/18/15 Pct Recovery = 79% Analysis Date = 05/13/15 Pct Recovery = 78% Analysis Date = 05/13/15 Pct Recovery = 78% Analysis Date = 05/08/15 Pct Recovery = 78% Analysis Date = 05/08/15 Pct Recovery = 78% Analysis Date = 05/03/15 Pct Recovery = 78% Analysis Date = 05/03/15 Pct Recovery = 78% Analysis Date = 04/28/15 Pct Recovery = 78% Analysis Date = 04/28/15 Pct Recovery = 78% Analysis Date = 04/23/15 Pct Recovery = 78% Analysis Date = 04/23/15 Pct Recovery = 78% Analysis Date = 04/18/15 Pct Recovery = 78% Analysis Date = 04/18/15 Pct Recovery = 78% Analysis Date = 04/13/15 Pct Recovery = 78% Analysis Date = 04/13/15 Pct Recovery = 78% Analysis Date = 04/08/15 Pct Recovery = 78% Analysis Date = 04/08/15 Pct Recovery = 78% Analysis Date = 04/03/15 Pct Recovery = 78% Analysis Date = 04/03/15 Pct Recovery = 78% Analysis Date = 03/29/15 Pct Recovery = 78% Analysis Date = 03/29/15 Pct Recovery = 78% Analysis Date = 03/24/15 Pct Recovery = 78% Analysis Date = 03/24/15 Pct Recovery = 78% Analysis Date = 03/19/15 Pct Recovery = 78% Analysis Date = 03/19/15 Pct Recovery = 78% Analysis Date = 03/14/15 Pct Recovery = 78% Analysis Date = 03/14/15 Pct Recovery = 78% Analysis Date = 03/09/15 Pct Recovery = 78% Analysis Date = 03/09/15 Pct Recovery = 78% Analysis Date = 03/04/15 Pct Recovery = 78% Analysis Date = 03/04/15 Pct Recovery = 78% Analysis Date = 02/27/15 Pct Recovery = 78% Analysis Date = 02/27/15 Pct Recovery = 78% Analysis Date = 02/22/15 Pct Recovery = 78% Analysis Date = 02/22/15 Pct Recovery = 78% Analysis Date = 02/17/15 Pct Recovery = 78% Analysis Date = 02/17/15 Pct Recovery = 78% Analysis Date = 02/12/15 Pct Recovery = 78% Analysis Date = 02/12/15 Pct Recovery = 78% Analysis Date = 02/07/15 Pct Recovery = 78% Analysis Date = 02/07/15 Pct Recovery = 78% Analysis Date = 02/02/15 Pct Recovery = 77% Analysis Date = 02/02/15 Pct Recovery = 77% Analysis Date = 01/28/15 Pct Recovery = 77% Analysis Date = 01/28/15 Pct Recovery = 77% Analysis Date = 01/23/15 Pct Recovery = 77% Analysis Date = 01/23/15 Pct Recovery = 77% Analysis Date = 01/18/15 Pct Recovery = 77% Analysis Date = 01/18/15 Pct Recovery = 77% Analysis Date = 01/13/15 Pct Recovery = 77% Analysis Date = 01/13/15 Pct Recovery = 77% Analysis Date = 01/08/15 Pct Recovery = 77% Analysis Date = 01/08/15 Pct Recovery = 77% Analysis Date = 01/03/15 Pct Recovery = 77% Analysis Date = 01/03/15 Pct Recovery = 77% Analysis Date = 12/29/14 Pct Recovery = 77% Analysis Date = 12/29/14 Pct Recovery = 77% Analysis Date = 12/24/14 Pct Recovery = 77% Analysis Date = 12/24/14 Pct Recovery = 77% Analysis Date = 12/19/14 Pct Recovery = 77% Analysis Date = 12/19/14 Pct Recovery = 77% Analysis Date = 12/14/14 Pct Recovery = 77% Analysis Date = 12/14/14 Pct Recovery = 77% Analysis Date = 12/09/14 Pct Recovery = 77% Analysis Date = 12/09/14 Pct Recovery = 77% Analysis Date = 12/04/14 Pct Recovery = 77% Analysis Date = 12/04/14 Pct Recovery = 77% Analysis Date = 11/29/14 Pct Recovery = 77% Analysis Date = 11/29/14 Pct Recovery = 77% Analysis Date = 11/24/14 Pct Recovery = 77% Analysis Date = 11/24/14 Pct Recovery = 77% Analysis Date = 11/19/14 Pct Recovery = 77% Analysis Date = 11/19/14 Pct Recovery = 77% Analysis Date = 11/14/14 Pct Recovery = 76% Analysis Date = 11/14/14 Pct Recovery = 76% Analysis Date = 11/09/14 Pct Recovery = 76% Analysis Date = 11/09/14 Pct Recovery = 76% Analysis Date = 11/04/14 Pct Recovery = 76% Analysis Date = 11/04/14 Pct Recovery = 76% Analysis Date = 10/30/14 Pct Recovery = 76% Analysis Date = 10/30/14 Pct Recovery = 76% Analysis Date = 10/25/14 Pct Recovery = 76% Analysis Date = 10/25/14 Pct Recovery = 76% Analysis Date = 10/20/14 Pct Recovery = 76% Analysis Date = 10/20/14 Pct Recovery = 76% Analysis Date = 10/15/14 Pct Recovery = 76% Analysis Date = 10/15/14 Pct Recovery = 76% Analysis Date = 10/10/14 Pct Recovery = 76% Analysis Date = 10/10/14 Pct Recovery = 76% Analysis Date = 10/05/14 Pct Recovery = 76% Analysis Date = 10/05/14 Pct Recovery = 76% Analysis Date = 09/30/14 Pct Recovery = 76% Analysis Date = 09/30/14 Pct Recovery = 76% Analysis Date = 09/25/14 Pct Recovery = 76% Analysis Date = 09/25/14 Pct Recovery = 76% Analysis Date = 09/20/14 Pct Recovery = 76% Analysis Date = 09/20/14 Pct Recovery = 76% Analysis Date = 09/15/14 Pct Recovery = 76% Analysis Date = 09/15/14 Pct Recovery = 76% Analysis Date = 09/10/14 Pct Recovery = 76% Analysis Date = 09/10/14 Pct Recovery = 76% Analysis Date = 09/05/14 Pct Recovery = 76% Analysis Date = 09/05/14 Pct Recovery = 76% Analysis Date = 08/31/14 Pct Recovery = 76% Analysis Date = 08/31/14 Pct Recovery = 76% Analysis Date = 08/26/14 Pct Recovery = 75% Analysis Date = 08/26/14 Pct Recovery = 75% Analysis Date = 08/21/14 Pct Recovery = 75% Analysis Date = 08/21/14 Pct Recovery = 75% Analysis Date = 08/16/14 Pct Recovery = 75% Analysis Date = 08/16/14 Pct Recovery = 75% Analysis Date = 08/11/14 Pct Recovery = 75% Analysis Date = 08/11/14 Pct Recovery = 75% Analysis Date = 08/06/14 Pct Recovery = 75% Analysis Date = 08/06/14 Pct Recovery = 75% Analysis Date = 08/01/14 Pct Recovery = 75% Analysis Date = 08/01/14 Pct Recovery = 75% Analysis Date = 07/27/14 Pct Recovery = 75% Analysis Date = 07/27/14 Pct Recovery = 75% Analysis Date = 07/22/14 Pct Recovery = 75% Analysis Date = 07/22/14 Pct Recovery = 75% Analysis Date = 07/17/14 Pct Recovery = 75% Analysis Date = 07/17/14 Pct Recovery = 75% Analysis Date = 07/12/14 Pct Recovery = 75% Analysis Date = 07/12/14 Pct Recovery = 75% Analysis Date = 07/07/14 Pct Recovery = 75% Analysis Date = 07/07/14 Pct Recovery = 75% Analysis Date = 07/02/14 Pct Recovery = 75% Analysis Date = 07/02/14 Pct Recovery = 75% Analysis Date = 06/27/14 Pct Recovery = 75% Analysis Date = 06/27/14 Pct Recovery = 75% Analysis Date = 06/22/14 Pct Recovery = 75% Analysis Date = 06/22/14 Pct Recovery = 75% Analysis Date = 06/17/14 Pct Recovery = 75% Analysis Date = 06/17/14 Pct Recovery = 75% Analysis Date = 06/12/14 Pct Recovery = 74% Analysis Date = 06/12/14 Pct Recovery = 74% Analysis Date = 06/07/14 Pct Recovery = 74% Analysis Date = 06/07/14 Pct Recovery = 74% Analysis Date = 06/02/14 Pct Recovery = 74% Analysis Date = 06/02/14 Pct Recovery = 74% Analysis Date = 05/28/14 Pct Recovery = 74% Analysis Date = 05/28/14 Pct Recovery = 74% Analysis Date = 05/23/14 Pct Recovery = 74% Analysis Date = 05/23/14 Pct Recovery = 74% Analysis Date = 05/18/14 Pct Recovery = 74% Analysis Date = 05/18/14 Pct Recovery = 74% Analysis Date = 05/13/14 Pct Recovery = 74% Analysis Date = 05/13/14 Pct Recovery = 74% Analysis Date = 05/08/14 Pct Recovery = 74% Analysis Date = 05/08/14 Pct Recovery = 74% Analysis Date = 05/03/14 Pct Recovery = 74% Analysis Date = 05/03/14 Pct Recovery = 74% Analysis Date = 04/28/14 Pct Recovery = 74% Analysis Date = 04/28/14 Pct Recovery = 74% Analysis Date = 04/23/14 Pct Recovery = 74% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
ATRAZINE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 2 70% 1% 70% 1%
>= Reporting Level 73 79% 12% 77% 10%
Total 75 79% 12% 77% 12%

Sample Statistics
ATRAZINE

Characteristic N % % Basis
Plotted 75 99% Spiked
Estimated Values 3 4% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 76 .  
False Negatives 1 1% 1 out of 76
Not Spiked 39 .  
False Positives 5 13% 5 out of 39

BQS OBSP Determination:
BENZTROPINE
METHOD: 2440 , TESTIDCODE: 67997LCM56
Open Data Set

Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 33% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 39% Analysis Date = 11/24/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 83% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 80 µl & Abs 051315: 80 µl Pct Recovery = 109% Analysis Date = 10/01/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 121% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 80 µl & ERA 0406-15-08: 80 µl Pct Recovery = 49% Analysis Date = 11/05/15 SpikeMix = ERA 0406-15-08: 80 µl & Abs 052215: 80 µl Pct Recovery = 69% Analysis Date = 11/18/16 SpikeMix = ERA 04281604: 80 µl & ERA 04281603: 80 µl Pct Recovery = 52% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & ERA 04281604: 80 µl Pct Recovery = 39% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 50% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 40% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 49% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 51% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 70% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 62% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 84% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 76% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-07A: 40 µl & Abs 051315: 40 µl Pct Recovery = 51% Analysis Date = 07/31/15 SpikeMix = Abs 051315: 40 µl & Abs 052215: 40 µl Pct Recovery = 55% Analysis Date = 07/30/15 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 63% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-08: 40 µl & Abs 052215: 40 µl Pct Recovery = 52% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 39% Analysis Date = 11/04/15 SpikeMix = ERA 0406-15-07A: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 59% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-08: 40 µl & ERA 0406-15-09: 40 µl Pct Recovery = 53% Analysis Date = 04/29/15 SpikeMix = ERA 0319-14-05: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 39% Analysis Date = 03/11/15 SpikeMix = ERA 0318-14-02: 15 µl & Abs 041714: 15 µl Pct Recovery = 41% Analysis Date = 02/06/15 SpikeMix = Abs 041814: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 41% Analysis Date = 12/06/14 SpikeMix = ERA 0318-14-02: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 42% Analysis Date = 10/11/14 SpikeMix = ERA 0318-14-02: 60 µl & ERA 0319-14-04: 60 µl Pct Recovery = 31% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 48% Analysis Date = 12/07/14 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 60% Analysis Date = 10/25/14 SpikeMix = Abs 041614: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 50% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 50% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 53% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 39% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 56% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 85% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 67% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 72% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 94% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 104% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 34% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 38% Analysis Date = 02/23/16 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 52% Analysis Date = 08/11/15 SpikeMix = Abs 050115: 20 µl & Abs 051315: 20 µl Pct Recovery = 29% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 104% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-08: 20 µl & ERA 0406-15-09: 20 µl Pct Recovery = 36% Analysis Date = 11/25/15 SpikeMix = Abs 050115: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 62% Analysis Date = 09/15/15 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 57% Analysis Date = 09/09/15 SpikeMix = ERA 0406-15-08: 20 µl & Abs 052215: 20 µl Pct Recovery = 71% Analysis Date = 12/07/14 SpikeMix = ERA 0318-14-02: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 54% Analysis Date = 04/30/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 39% Analysis Date = 10/24/14 SpikeMix = ERA 0319-14-05: 8 µl & Abs 041614: 8 µl Pct Recovery = 38% Analysis Date = 04/09/16 SpikeMix = Abs 051315: 10 µl & ERA 0406-15-09: 10 µl Pct Recovery = 173% Analysis Date = 01/18/17 Pct Recovery = 46% Analysis Date = 01/14/17 Pct Recovery = 47% Analysis Date = 01/14/17 Pct Recovery = 47% Analysis Date = 01/10/17 Pct Recovery = 47% Analysis Date = 01/10/17 Pct Recovery = 47% Analysis Date = 01/06/17 Pct Recovery = 48% Analysis Date = 01/06/17 Pct Recovery = 48% Analysis Date = 01/02/17 Pct Recovery = 48% Analysis Date = 01/02/17 Pct Recovery = 48% Analysis Date = 12/29/16 Pct Recovery = 49% Analysis Date = 12/29/16 Pct Recovery = 49% Analysis Date = 12/25/16 Pct Recovery = 49% Analysis Date = 12/25/16 Pct Recovery = 49% Analysis Date = 12/20/16 Pct Recovery = 50% Analysis Date = 12/20/16 Pct Recovery = 50% Analysis Date = 12/16/16 Pct Recovery = 50% Analysis Date = 12/16/16 Pct Recovery = 50% Analysis Date = 12/12/16 Pct Recovery = 51% Analysis Date = 12/12/16 Pct Recovery = 51% Analysis Date = 12/08/16 Pct Recovery = 51% Analysis Date = 12/08/16 Pct Recovery = 51% Analysis Date = 12/04/16 Pct Recovery = 52% Analysis Date = 12/04/16 Pct Recovery = 52% Analysis Date = 11/30/16 Pct Recovery = 52% Analysis Date = 11/30/16 Pct Recovery = 52% Analysis Date = 11/25/16 Pct Recovery = 53% Analysis Date = 11/25/16 Pct Recovery = 53% Analysis Date = 11/21/16 Pct Recovery = 53% Analysis Date = 11/21/16 Pct Recovery = 53% Analysis Date = 11/17/16 Pct Recovery = 53% Analysis Date = 11/17/16 Pct Recovery = 53% Analysis Date = 11/13/16 Pct Recovery = 54% Analysis Date = 11/13/16 Pct Recovery = 54% Analysis Date = 11/09/16 Pct Recovery = 54% Analysis Date = 11/09/16 Pct Recovery = 54% Analysis Date = 11/05/16 Pct Recovery = 55% Analysis Date = 11/05/16 Pct Recovery = 55% Analysis Date = 11/01/16 Pct Recovery = 55% Analysis Date = 11/01/16 Pct Recovery = 55% Analysis Date = 10/27/16 Pct Recovery = 56% Analysis Date = 10/27/16 Pct Recovery = 56% Analysis Date = 10/23/16 Pct Recovery = 56% Analysis Date = 10/23/16 Pct Recovery = 56% Analysis Date = 10/19/16 Pct Recovery = 57% Analysis Date = 10/19/16 Pct Recovery = 57% Analysis Date = 10/15/16 Pct Recovery = 57% Analysis Date = 10/15/16 Pct Recovery = 57% Analysis Date = 10/11/16 Pct Recovery = 58% Analysis Date = 10/11/16 Pct Recovery = 58% Analysis Date = 10/07/16 Pct Recovery = 58% Analysis Date = 10/07/16 Pct Recovery = 58% Analysis Date = 10/02/16 Pct Recovery = 59% Analysis Date = 10/02/16 Pct Recovery = 59% Analysis Date = 09/28/16 Pct Recovery = 59% Analysis Date = 09/28/16 Pct Recovery = 59% Analysis Date = 09/24/16 Pct Recovery = 60% Analysis Date = 09/24/16 Pct Recovery = 60% Analysis Date = 09/20/16 Pct Recovery = 60% Analysis Date = 09/20/16 Pct Recovery = 60% Analysis Date = 09/16/16 Pct Recovery = 61% Analysis Date = 09/16/16 Pct Recovery = 61% Analysis Date = 09/12/16 Pct Recovery = 61% Analysis Date = 09/12/16 Pct Recovery = 61% Analysis Date = 09/08/16 Pct Recovery = 62% Analysis Date = 09/08/16 Pct Recovery = 62% Analysis Date = 09/03/16 Pct Recovery = 62% Analysis Date = 09/03/16 Pct Recovery = 62% Analysis Date = 08/30/16 Pct Recovery = 63% Analysis Date = 08/30/16 Pct Recovery = 63% Analysis Date = 08/26/16 Pct Recovery = 63% Analysis Date = 08/26/16 Pct Recovery = 63% Analysis Date = 08/22/16 Pct Recovery = 64% Analysis Date = 08/22/16 Pct Recovery = 64% Analysis Date = 08/18/16 Pct Recovery = 64% Analysis Date = 08/18/16 Pct Recovery = 64% Analysis Date = 08/14/16 Pct Recovery = 64% Analysis Date = 08/14/16 Pct Recovery = 64% Analysis Date = 08/09/16 Pct Recovery = 65% Analysis Date = 08/09/16 Pct Recovery = 65% Analysis Date = 08/05/16 Pct Recovery = 65% Analysis Date = 08/05/16 Pct Recovery = 65% Analysis Date = 08/01/16 Pct Recovery = 66% Analysis Date = 08/01/16 Pct Recovery = 66% Analysis Date = 07/28/16 Pct Recovery = 66% Analysis Date = 07/28/16 Pct Recovery = 66% Analysis Date = 07/24/16 Pct Recovery = 67% Analysis Date = 07/24/16 Pct Recovery = 67% Analysis Date = 07/20/16 Pct Recovery = 67% Analysis Date = 07/20/16 Pct Recovery = 67% Analysis Date = 07/16/16 Pct Recovery = 67% Analysis Date = 07/16/16 Pct Recovery = 67% Analysis Date = 07/11/16 Pct Recovery = 67% Analysis Date = 07/11/16 Pct Recovery = 67% Analysis Date = 07/07/16 Pct Recovery = 67% Analysis Date = 07/07/16 Pct Recovery = 67% Analysis Date = 07/03/16 Pct Recovery = 67% Analysis Date = 07/03/16 Pct Recovery = 67% Analysis Date = 06/29/16 Pct Recovery = 68% Analysis Date = 06/29/16 Pct Recovery = 68% Analysis Date = 06/25/16 Pct Recovery = 68% Analysis Date = 06/25/16 Pct Recovery = 68% Analysis Date = 06/21/16 Pct Recovery = 68% Analysis Date = 06/21/16 Pct Recovery = 68% Analysis Date = 06/16/16 Pct Recovery = 68% Analysis Date = 06/16/16 Pct Recovery = 68% Analysis Date = 06/12/16 Pct Recovery = 68% Analysis Date = 06/12/16 Pct Recovery = 68% Analysis Date = 06/08/16 Pct Recovery = 68% Analysis Date = 06/08/16 Pct Recovery = 68% Analysis Date = 06/04/16 Pct Recovery = 68% Analysis Date = 06/04/16 Pct Recovery = 68% Analysis Date = 05/31/16 Pct Recovery = 68% Analysis Date = 05/31/16 Pct Recovery = 68% Analysis Date = 05/27/16 Pct Recovery = 69% Analysis Date = 05/27/16 Pct Recovery = 69% Analysis Date = 05/23/16 Pct Recovery = 69% Analysis Date = 05/23/16 Pct Recovery = 69% Analysis Date = 05/18/16 Pct Recovery = 69% Analysis Date = 05/18/16 Pct Recovery = 69% Analysis Date = 05/14/16 Pct Recovery = 69% Analysis Date = 05/14/16 Pct Recovery = 69% Analysis Date = 05/10/16 Pct Recovery = 69% Analysis Date = 05/10/16 Pct Recovery = 69% Analysis Date = 05/06/16 Pct Recovery = 69% Analysis Date = 05/06/16 Pct Recovery = 69% Analysis Date = 05/02/16 Pct Recovery = 69% Analysis Date = 05/02/16 Pct Recovery = 69% Analysis Date = 04/28/16 Pct Recovery = 69% Analysis Date = 04/28/16 Pct Recovery = 69% Analysis Date = 04/23/16 Pct Recovery = 70% Analysis Date = 04/23/16 Pct Recovery = 70% Analysis Date = 04/19/16 Pct Recovery = 70% Analysis Date = 04/19/16 Pct Recovery = 70% Analysis Date = 04/15/16 Pct Recovery = 70% Analysis Date = 04/15/16 Pct Recovery = 70% Analysis Date = 04/11/16 Pct Recovery = 70% Analysis Date = 04/11/16 Pct Recovery = 70% Analysis Date = 04/07/16 Pct Recovery = 70% Analysis Date = 04/07/16 Pct Recovery = 70% Analysis Date = 04/03/16 Pct Recovery = 70% Analysis Date = 04/03/16 Pct Recovery = 70% Analysis Date = 03/29/16 Pct Recovery = 71% Analysis Date = 03/29/16 Pct Recovery = 71% Analysis Date = 03/25/16 Pct Recovery = 71% Analysis Date = 03/25/16 Pct Recovery = 71% Analysis Date = 03/21/16 Pct Recovery = 71% Analysis Date = 03/21/16 Pct Recovery = 71% Analysis Date = 03/17/16 Pct Recovery = 72% Analysis Date = 03/17/16 Pct Recovery = 72% Analysis Date = 03/13/16 Pct Recovery = 72% Analysis Date = 03/13/16 Pct Recovery = 72% Analysis Date = 03/09/16 Pct Recovery = 72% Analysis Date = 03/09/16 Pct Recovery = 72% Analysis Date = 03/05/16 Pct Recovery = 72% Analysis Date = 03/05/16 Pct Recovery = 72% Analysis Date = 02/29/16 Pct Recovery = 73% Analysis Date = 02/29/16 Pct Recovery = 73% Analysis Date = 02/25/16 Pct Recovery = 73% Analysis Date = 02/25/16 Pct Recovery = 73% Analysis Date = 02/21/16 Pct Recovery = 73% Analysis Date = 02/21/16 Pct Recovery = 73% Analysis Date = 02/17/16 Pct Recovery = 73% Analysis Date = 02/17/16 Pct Recovery = 73% Analysis Date = 02/13/16 Pct Recovery = 73% Analysis Date = 02/13/16 Pct Recovery = 73% Analysis Date = 02/09/16 Pct Recovery = 72% Analysis Date = 02/09/16 Pct Recovery = 72% Analysis Date = 02/04/16 Pct Recovery = 72% Analysis Date = 02/04/16 Pct Recovery = 72% Analysis Date = 01/31/16 Pct Recovery = 72% Analysis Date = 01/31/16 Pct Recovery = 72% Analysis Date = 01/27/16 Pct Recovery = 71% Analysis Date = 01/27/16 Pct Recovery = 71% Analysis Date = 01/23/16 Pct Recovery = 71% Analysis Date = 01/23/16 Pct Recovery = 71% Analysis Date = 01/19/16 Pct Recovery = 71% Analysis Date = 01/19/16 Pct Recovery = 71% Analysis Date = 01/15/16 Pct Recovery = 71% Analysis Date = 01/15/16 Pct Recovery = 71% Analysis Date = 01/11/16 Pct Recovery = 70% Analysis Date = 01/11/16 Pct Recovery = 70% Analysis Date = 01/06/16 Pct Recovery = 70% Analysis Date = 01/06/16 Pct Recovery = 70% Analysis Date = 01/02/16 Pct Recovery = 70% Analysis Date = 01/02/16 Pct Recovery = 70% Analysis Date = 12/29/15 Pct Recovery = 70% Analysis Date = 12/29/15 Pct Recovery = 70% Analysis Date = 12/25/15 Pct Recovery = 69% Analysis Date = 12/25/15 Pct Recovery = 69% Analysis Date = 12/21/15 Pct Recovery = 69% Analysis Date = 12/21/15 Pct Recovery = 69% Analysis Date = 12/17/15 Pct Recovery = 69% Analysis Date = 12/17/15 Pct Recovery = 69% Analysis Date = 12/12/15 Pct Recovery = 68% Analysis Date = 12/12/15 Pct Recovery = 68% Analysis Date = 12/08/15 Pct Recovery = 68% Analysis Date = 12/08/15 Pct Recovery = 68% Analysis Date = 12/04/15 Pct Recovery = 68% Analysis Date = 12/04/15 Pct Recovery = 68% Analysis Date = 11/30/15 Pct Recovery = 68% Analysis Date = 11/30/15 Pct Recovery = 68% Analysis Date = 11/26/15 Pct Recovery = 67% Analysis Date = 11/26/15 Pct Recovery = 67% Analysis Date = 11/22/15 Pct Recovery = 67% Analysis Date = 11/22/15 Pct Recovery = 67% Analysis Date = 11/18/15 Pct Recovery = 67% Analysis Date = 11/18/15 Pct Recovery = 67% Analysis Date = 11/13/15 Pct Recovery = 66% Analysis Date = 11/13/15 Pct Recovery = 66% Analysis Date = 11/09/15 Pct Recovery = 66% Analysis Date = 11/09/15 Pct Recovery = 66% Analysis Date = 11/05/15 Pct Recovery = 66% Analysis Date = 11/05/15 Pct Recovery = 66% Analysis Date = 11/01/15 Pct Recovery = 66% Analysis Date = 11/01/15 Pct Recovery = 66% Analysis Date = 10/28/15 Pct Recovery = 65% Analysis Date = 10/28/15 Pct Recovery = 65% Analysis Date = 10/24/15 Pct Recovery = 65% Analysis Date = 10/24/15 Pct Recovery = 65% Analysis Date = 10/19/15 Pct Recovery = 64% Analysis Date = 10/19/15 Pct Recovery = 64% Analysis Date = 10/15/15 Pct Recovery = 64% Analysis Date = 10/15/15 Pct Recovery = 64% Analysis Date = 10/11/15 Pct Recovery = 63% Analysis Date = 10/11/15 Pct Recovery = 63% Analysis Date = 10/07/15 Pct Recovery = 63% Analysis Date = 10/07/15 Pct Recovery = 63% Analysis Date = 10/03/15 Pct Recovery = 63% Analysis Date = 10/03/15 Pct Recovery = 63% Analysis Date = 09/29/15 Pct Recovery = 62% Analysis Date = 09/29/15 Pct Recovery = 62% Analysis Date = 09/25/15 Pct Recovery = 62% Analysis Date = 09/25/15 Pct Recovery = 62% Analysis Date = 09/20/15 Pct Recovery = 62% Analysis Date = 09/20/15 Pct Recovery = 62% Analysis Date = 09/16/15 Pct Recovery = 61% Analysis Date = 09/16/15 Pct Recovery = 61% Analysis Date = 09/12/15 Pct Recovery = 61% Analysis Date = 09/12/15 Pct Recovery = 61% Analysis Date = 09/08/15 Pct Recovery = 61% Analysis Date = 09/08/15 Pct Recovery = 61% Analysis Date = 09/04/15 Pct Recovery = 60% Analysis Date = 09/04/15 Pct Recovery = 60% Analysis Date = 08/31/15 Pct Recovery = 60% Analysis Date = 08/31/15 Pct Recovery = 60% Analysis Date = 08/26/15 Pct Recovery = 60% Analysis Date = 08/26/15 Pct Recovery = 60% Analysis Date = 08/22/15 Pct Recovery = 59% Analysis Date = 08/22/15 Pct Recovery = 59% Analysis Date = 08/18/15 Pct Recovery = 59% Analysis Date = 08/18/15 Pct Recovery = 59% Analysis Date = 08/14/15 Pct Recovery = 59% Analysis Date = 08/14/15 Pct Recovery = 59% Analysis Date = 08/10/15 Pct Recovery = 58% Analysis Date = 08/10/15 Pct Recovery = 58% Analysis Date = 08/06/15 Pct Recovery = 58% Analysis Date = 08/06/15 Pct Recovery = 58% Analysis Date = 08/02/15 Pct Recovery = 58% Analysis Date = 08/02/15 Pct Recovery = 58% Analysis Date = 07/28/15 Pct Recovery = 58% Analysis Date = 07/28/15 Pct Recovery = 58% Analysis Date = 07/24/15 Pct Recovery = 58% Analysis Date = 07/24/15 Pct Recovery = 58% Analysis Date = 07/20/15 Pct Recovery = 57% Analysis Date = 07/20/15 Pct Recovery = 57% Analysis Date = 07/16/15 Pct Recovery = 57% Analysis Date = 07/16/15 Pct Recovery = 57% Analysis Date = 07/12/15 Pct Recovery = 57% Analysis Date = 07/12/15 Pct Recovery = 57% Analysis Date = 07/08/15 Pct Recovery = 57% Analysis Date = 07/08/15 Pct Recovery = 57% Analysis Date = 07/03/15 Pct Recovery = 56% Analysis Date = 07/03/15 Pct Recovery = 56% Analysis Date = 06/29/15 Pct Recovery = 56% Analysis Date = 06/29/15 Pct Recovery = 56% Analysis Date = 06/25/15 Pct Recovery = 56% Analysis Date = 06/25/15 Pct Recovery = 56% Analysis Date = 06/21/15 Pct Recovery = 56% Analysis Date = 06/21/15 Pct Recovery = 56% Analysis Date = 06/17/15 Pct Recovery = 55% Analysis Date = 06/17/15 Pct Recovery = 55% Analysis Date = 06/13/15 Pct Recovery = 55% Analysis Date = 06/13/15 Pct Recovery = 55% Analysis Date = 06/08/15 Pct Recovery = 55% Analysis Date = 06/08/15 Pct Recovery = 55% Analysis Date = 06/04/15 Pct Recovery = 55% Analysis Date = 06/04/15 Pct Recovery = 55% Analysis Date = 05/31/15 Pct Recovery = 55% Analysis Date = 05/31/15 Pct Recovery = 55% Analysis Date = 05/27/15 Pct Recovery = 54% Analysis Date = 05/27/15 Pct Recovery = 54% Analysis Date = 05/23/15 Pct Recovery = 54% Analysis Date = 05/23/15 Pct Recovery = 54% Analysis Date = 05/19/15 Pct Recovery = 54% Analysis Date = 05/19/15 Pct Recovery = 54% Analysis Date = 05/15/15 Pct Recovery = 54% Analysis Date = 05/15/15 Pct Recovery = 54% Analysis Date = 05/10/15 Pct Recovery = 53% Analysis Date = 05/10/15 Pct Recovery = 53% Analysis Date = 05/06/15 Pct Recovery = 53% Analysis Date = 05/06/15 Pct Recovery = 53% Analysis Date = 05/02/15 Pct Recovery = 53% Analysis Date = 05/02/15 Pct Recovery = 53% Analysis Date = 04/28/15 Pct Recovery = 53% Analysis Date = 04/28/15 Pct Recovery = 53% Analysis Date = 04/24/15 Pct Recovery = 52% Analysis Date = 04/24/15 Pct Recovery = 52% Analysis Date = 04/20/15 Pct Recovery = 52% Analysis Date = 04/20/15 Pct Recovery = 52% Analysis Date = 04/15/15 Pct Recovery = 52% Analysis Date = 04/15/15 Pct Recovery = 52% Analysis Date = 04/11/15 Pct Recovery = 52% Analysis Date = 04/11/15 Pct Recovery = 52% Analysis Date = 04/07/15 Pct Recovery = 51% Analysis Date = 04/07/15 Pct Recovery = 51% Analysis Date = 04/03/15 Pct Recovery = 51% Analysis Date = 04/03/15 Pct Recovery = 51% Analysis Date = 03/30/15 Pct Recovery = 51% Analysis Date = 03/30/15 Pct Recovery = 51% Analysis Date = 03/26/15 Pct Recovery = 50% Analysis Date = 03/26/15 Pct Recovery = 50% Analysis Date = 03/22/15 Pct Recovery = 50% Analysis Date = 03/22/15 Pct Recovery = 50% Analysis Date = 03/17/15 Pct Recovery = 50% Analysis Date = 03/17/15 Pct Recovery = 50% Analysis Date = 03/13/15 Pct Recovery = 50% Analysis Date = 03/13/15 Pct Recovery = 50% Analysis Date = 03/09/15 Pct Recovery = 49% Analysis Date = 03/09/15 Pct Recovery = 49% Analysis Date = 03/05/15 Pct Recovery = 49% Analysis Date = 03/05/15 Pct Recovery = 49% Analysis Date = 03/01/15 Pct Recovery = 49% Analysis Date = 03/01/15 Pct Recovery = 49% Analysis Date = 02/25/15 Pct Recovery = 49% Analysis Date = 02/25/15 Pct Recovery = 49% Analysis Date = 02/20/15 Pct Recovery = 48% Analysis Date = 02/20/15 Pct Recovery = 48% Analysis Date = 02/16/15 Pct Recovery = 48% Analysis Date = 02/16/15 Pct Recovery = 48% Analysis Date = 02/12/15 Pct Recovery = 48% Analysis Date = 02/12/15 Pct Recovery = 48% Analysis Date = 02/08/15 Pct Recovery = 47% Analysis Date = 02/08/15 Pct Recovery = 47% Analysis Date = 02/04/15 Pct Recovery = 47% Analysis Date = 02/04/15 Pct Recovery = 47% Analysis Date = 01/31/15 Pct Recovery = 47% Analysis Date = 01/31/15 Pct Recovery = 47% Analysis Date = 01/27/15 Pct Recovery = 47% Analysis Date = 01/27/15 Pct Recovery = 47% Analysis Date = 01/22/15 Pct Recovery = 46% Analysis Date = 01/22/15 Pct Recovery = 46% Analysis Date = 01/18/15 Pct Recovery = 46% Analysis Date = 01/18/15 Pct Recovery = 46% Analysis Date = 01/14/15 Pct Recovery = 46% Analysis Date = 01/14/15 Pct Recovery = 46% Analysis Date = 01/10/15 Pct Recovery = 45% Analysis Date = 01/10/15 Pct Recovery = 45% Analysis Date = 01/06/15 Pct Recovery = 45% Analysis Date = 01/06/15 Pct Recovery = 45% Analysis Date = 01/02/15 Pct Recovery = 45% Analysis Date = 01/02/15 Pct Recovery = 45% Analysis Date = 12/28/14 Pct Recovery = 45% Analysis Date = 12/28/14 Pct Recovery = 45% Analysis Date = 12/24/14 Pct Recovery = 44% Analysis Date = 12/24/14 Pct Recovery = 44% Analysis Date = 12/20/14 Pct Recovery = 44% Analysis Date = 12/20/14 Pct Recovery = 44% Analysis Date = 12/16/14 Pct Recovery = 44% Analysis Date = 12/16/14 Pct Recovery = 44% Analysis Date = 12/12/14 Pct Recovery = 43% Analysis Date = 12/12/14 Pct Recovery = 43% Analysis Date = 12/08/14 Pct Recovery = 43% Analysis Date = 12/08/14 Pct Recovery = 43% Analysis Date = 12/04/14 Pct Recovery = 43% Analysis Date = 12/04/14 Pct Recovery = 43% Analysis Date = 11/29/14 Pct Recovery = 43% Analysis Date = 11/29/14 Pct Recovery = 43% Analysis Date = 11/25/14 Pct Recovery = 42% Analysis Date = 11/25/14 Pct Recovery = 42% Analysis Date = 11/21/14 Pct Recovery = 42% Analysis Date = 11/21/14 Pct Recovery = 42% Analysis Date = 11/17/14 Pct Recovery = 42% Analysis Date = 11/17/14 Pct Recovery = 42% Analysis Date = 11/13/14 Pct Recovery = 42% Analysis Date = 11/13/14 Pct Recovery = 42% Analysis Date = 11/09/14 Pct Recovery = 41% Analysis Date = 11/09/14 Pct Recovery = 41% Analysis Date = 11/04/14 Pct Recovery = 41% Analysis Date = 11/04/14 Pct Recovery = 41% Analysis Date = 10/31/14 Pct Recovery = 41% Analysis Date = 10/31/14 Pct Recovery = 41% Analysis Date = 10/27/14 Pct Recovery = 40% Analysis Date = 10/27/14 Pct Recovery = 40% Analysis Date = 10/23/14 Pct Recovery = 40% Analysis Date = 10/23/14 Pct Recovery = 40% Analysis Date = 10/19/14 Pct Recovery = 40% Analysis Date = 10/19/14 Pct Recovery = 40% Analysis Date = 10/15/14 Pct Recovery = 40% Analysis Date = 10/15/14 Pct Recovery = 40% Analysis Date = 10/11/14 Pct Recovery = 39% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
BENZTROPINE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 1 173% . 173% 0%
>= Reporting Level 53 57% 21% 52% 20%
Total 54 59% 26% 52% 22%

Sample Statistics
BENZTROPINE

Characteristic N % % Basis
Plotted 54 72% Spiked
Estimated Values 54 72% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 3 4% Spiked
Spiked 75 .  
False Negatives 18 24% 18 out of 75
Not Spiked 40 .  
False Positives 0 0% 0 out of 40

BQS OBSP Determination:
BETAMETHASONE
METHOD: 2440 , TESTIDCODE: 67485LCM56
Open Data Set

Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 87% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 85% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 80 µl & ERA 0406-15-08: 80 µl Pct Recovery = 71% Analysis Date = 11/05/15 SpikeMix = ERA 0406-15-08: 80 µl & Abs 052215: 80 µl Pct Recovery = 75% Analysis Date = 11/24/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 83% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 80 µl & Abs 051315: 80 µl Pct Recovery = 82% Analysis Date = 10/01/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 44% Analysis Date = 09/24/16 SpikeMix = Crescent EN160610015: 80 µl & Abs 061416: 80 µl Pct Recovery = 84% Analysis Date = 09/24/16 SpikeMix = Abs 061416: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 88% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 92% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 91% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 89% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 75% Analysis Date = 11/18/16 SpikeMix = ERA 04281604: 80 µl & ERA 04281603: 80 µl Pct Recovery = 73% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & ERA 04281604: 80 µl Pct Recovery = 72% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 119% Analysis Date = 12/07/14 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 113% Analysis Date = 10/25/14 SpikeMix = Abs 041614: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 108% Analysis Date = 06/22/14 SpikeMix = Abs 041814: 60 µl & Abs 041614: 60 µl Pct Recovery = 88% Analysis Date = 06/11/14 SpikeMix = Abs 041614: 60 µl & Abs 041714: 60 µl Pct Recovery = 98% Analysis Date = 04/29/15 SpikeMix = ERA 0319-14-05: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 94% Analysis Date = 03/11/15 SpikeMix = ERA 0318-14-02: 15 µl & Abs 041714: 15 µl Pct Recovery = 113% Analysis Date = 02/06/15 SpikeMix = Abs 041814: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 122% Analysis Date = 12/06/14 SpikeMix = ERA 0318-14-02: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 89% Analysis Date = 10/11/14 SpikeMix = ERA 0318-14-02: 60 µl & ERA 0319-14-04: 60 µl Pct Recovery = 84% Analysis Date = 08/21/14 SpikeMix = ERA 0318-14-02: 60 µl & Abs 041714: 60 µl Pct Recovery = 89% Analysis Date = 07/26/14 SpikeMix = ERA 0319-14-05: 60 µl & ERA 0318-14-02: 60 µl Pct Recovery = 88% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-08: 40 µl & Abs 052215: 40 µl Pct Recovery = 35% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 75% Analysis Date = 11/04/15 SpikeMix = ERA 0406-15-07A: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 71% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-08: 40 µl & ERA 0406-15-09: 40 µl Pct Recovery = 86% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 96% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 78% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-07A: 40 µl & Abs 051315: 40 µl Pct Recovery = 89% Analysis Date = 07/31/15 SpikeMix = Abs 051315: 40 µl & Abs 052215: 40 µl Pct Recovery = 73% Analysis Date = 07/30/15 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 104% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 74% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 77% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 75% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 70% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 70% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 64% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 66% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 64% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 105% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 134% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 91% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 88% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 78% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 90% Analysis Date = 04/30/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 70% Analysis Date = 02/10/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 105% Analysis Date = 10/24/14 SpikeMix = ERA 0319-14-05: 8 µl & Abs 041614: 8 µl Pct Recovery = 94% Analysis Date = 12/07/14 SpikeMix = ERA 0318-14-02: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 100% Analysis Date = 11/04/14 SpikeMix = Abs 041814: 8 µl & ERA 0318-14-02: 8 µl Pct Recovery = 116% Analysis Date = 09/12/14 SpikeMix = Abs 041614: 30 µl & ERA 0319-14-04: 30 µl Pct Recovery = 95% Analysis Date = 07/13/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 109% Analysis Date = 06/28/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 81% Analysis Date = 05/30/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 114% Analysis Date = 05/17/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 88% Analysis Date = 10/10/14 SpikeMix = Abs 041814: 30 µl & ERA 0318-14-02: 30 µl Pct Recovery = 114% Analysis Date = 08/30/14 SpikeMix = ERA 0318-14-02: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 100% Analysis Date = 07/20/14 SpikeMix = ERA 0318-14-02: 30 µl & Abs 041714: 30 µl Pct Recovery = 81% Analysis Date = 04/27/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 105% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 113% Analysis Date = 11/25/15 SpikeMix = Abs 050115: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 73% Analysis Date = 09/15/15 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 87% Analysis Date = 09/09/15 SpikeMix = ERA 0406-15-08: 20 µl & Abs 052215: 20 µl Pct Recovery = 71% Analysis Date = 02/23/16 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 70% Analysis Date = 08/11/15 SpikeMix = Abs 050115: 20 µl & Abs 051315: 20 µl Pct Recovery = 74% Analysis Date = 06/26/15 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 71% Analysis Date = 06/09/15 SpikeMix = Abs 051315: 20 µl & Abs 050115: 20 µl Pct Recovery = 100% Analysis Date = 04/09/16 SpikeMix = Abs 051315: 10 µl & ERA 0406-15-09: 10 µl Pct Recovery = 24% Analysis Date = 04/09/16 SpikeMix = Abs 051315: 10 µl & ERA 0406-15-09: 10 µl Pct Recovery = 44% Analysis Date = 01/04/17 Pct Recovery = 90% Analysis Date = 12/31/16 Pct Recovery = 90% Analysis Date = 12/31/16 Pct Recovery = 90% Analysis Date = 12/26/16 Pct Recovery = 89% Analysis Date = 12/26/16 Pct Recovery = 89% Analysis Date = 12/21/16 Pct Recovery = 89% Analysis Date = 12/21/16 Pct Recovery = 89% Analysis Date = 12/16/16 Pct Recovery = 89% Analysis Date = 12/16/16 Pct Recovery = 89% Analysis Date = 12/11/16 Pct Recovery = 88% Analysis Date = 12/11/16 Pct Recovery = 88% Analysis Date = 12/07/16 Pct Recovery = 88% Analysis Date = 12/07/16 Pct Recovery = 88% Analysis Date = 12/02/16 Pct Recovery = 88% Analysis Date = 12/02/16 Pct Recovery = 88% Analysis Date = 11/27/16 Pct Recovery = 87% Analysis Date = 11/27/16 Pct Recovery = 87% Analysis Date = 11/22/16 Pct Recovery = 87% Analysis Date = 11/22/16 Pct Recovery = 87% Analysis Date = 11/17/16 Pct Recovery = 87% Analysis Date = 11/17/16 Pct Recovery = 87% Analysis Date = 11/12/16 Pct Recovery = 86% Analysis Date = 11/12/16 Pct Recovery = 86% Analysis Date = 11/08/16 Pct Recovery = 86% Analysis Date = 11/08/16 Pct Recovery = 86% Analysis Date = 11/03/16 Pct Recovery = 86% Analysis Date = 11/03/16 Pct Recovery = 86% Analysis Date = 10/29/16 Pct Recovery = 85% Analysis Date = 10/29/16 Pct Recovery = 85% Analysis Date = 10/24/16 Pct Recovery = 85% Analysis Date = 10/24/16 Pct Recovery = 85% Analysis Date = 10/19/16 Pct Recovery = 84% Analysis Date = 10/19/16 Pct Recovery = 84% Analysis Date = 10/15/16 Pct Recovery = 84% Analysis Date = 10/15/16 Pct Recovery = 84% Analysis Date = 10/10/16 Pct Recovery = 84% Analysis Date = 10/10/16 Pct Recovery = 84% Analysis Date = 10/05/16 Pct Recovery = 83% Analysis Date = 10/05/16 Pct Recovery = 83% Analysis Date = 09/30/16 Pct Recovery = 83% Analysis Date = 09/30/16 Pct Recovery = 83% Analysis Date = 09/25/16 Pct Recovery = 83% Analysis Date = 09/25/16 Pct Recovery = 83% Analysis Date = 09/20/16 Pct Recovery = 82% Analysis Date = 09/20/16 Pct Recovery = 82% Analysis Date = 09/16/16 Pct Recovery = 82% Analysis Date = 09/16/16 Pct Recovery = 82% Analysis Date = 09/11/16 Pct Recovery = 82% Analysis Date = 09/11/16 Pct Recovery = 82% Analysis Date = 09/06/16 Pct Recovery = 81% Analysis Date = 09/06/16 Pct Recovery = 81% Analysis Date = 09/01/16 Pct Recovery = 81% Analysis Date = 09/01/16 Pct Recovery = 81% Analysis Date = 08/27/16 Pct Recovery = 81% Analysis Date = 08/27/16 Pct Recovery = 81% Analysis Date = 08/23/16 Pct Recovery = 80% Analysis Date = 08/23/16 Pct Recovery = 80% Analysis Date = 08/18/16 Pct Recovery = 80% Analysis Date = 08/18/16 Pct Recovery = 80% Analysis Date = 08/13/16 Pct Recovery = 80% Analysis Date = 08/13/16 Pct Recovery = 80% Analysis Date = 08/08/16 Pct Recovery = 79% Analysis Date = 08/08/16 Pct Recovery = 79% Analysis Date = 08/03/16 Pct Recovery = 79% Analysis Date = 08/03/16 Pct Recovery = 79% Analysis Date = 07/29/16 Pct Recovery = 79% Analysis Date = 07/29/16 Pct Recovery = 79% Analysis Date = 07/25/16 Pct Recovery = 78% Analysis Date = 07/25/16 Pct Recovery = 78% Analysis Date = 07/20/16 Pct Recovery = 78% Analysis Date = 07/20/16 Pct Recovery = 78% Analysis Date = 07/15/16 Pct Recovery = 78% Analysis Date = 07/15/16 Pct Recovery = 78% Analysis Date = 07/10/16 Pct Recovery = 78% Analysis Date = 07/10/16 Pct Recovery = 78% Analysis Date = 07/05/16 Pct Recovery = 78% Analysis Date = 07/05/16 Pct Recovery = 78% Analysis Date = 07/01/16 Pct Recovery = 78% Analysis Date = 07/01/16 Pct Recovery = 78% Analysis Date = 06/26/16 Pct Recovery = 77% Analysis Date = 06/26/16 Pct Recovery = 77% Analysis Date = 06/21/16 Pct Recovery = 77% Analysis Date = 06/21/16 Pct Recovery = 77% Analysis Date = 06/16/16 Pct Recovery = 77% Analysis Date = 06/16/16 Pct Recovery = 77% Analysis Date = 06/11/16 Pct Recovery = 77% Analysis Date = 06/11/16 Pct Recovery = 77% Analysis Date = 06/06/16 Pct Recovery = 77% Analysis Date = 06/06/16 Pct Recovery = 77% Analysis Date = 06/02/16 Pct Recovery = 76% Analysis Date = 06/02/16 Pct Recovery = 76% Analysis Date = 05/28/16 Pct Recovery = 76% Analysis Date = 05/28/16 Pct Recovery = 76% Analysis Date = 05/23/16 Pct Recovery = 76% Analysis Date = 05/23/16 Pct Recovery = 76% Analysis Date = 05/18/16 Pct Recovery = 76% Analysis Date = 05/18/16 Pct Recovery = 76% Analysis Date = 05/13/16 Pct Recovery = 76% Analysis Date = 05/13/16 Pct Recovery = 76% Analysis Date = 05/08/16 Pct Recovery = 76% Analysis Date = 05/08/16 Pct Recovery = 76% Analysis Date = 05/04/16 Pct Recovery = 75% Analysis Date = 05/04/16 Pct Recovery = 75% Analysis Date = 04/29/16 Pct Recovery = 75% Analysis Date = 04/29/16 Pct Recovery = 75% Analysis Date = 04/24/16 Pct Recovery = 75% Analysis Date = 04/24/16 Pct Recovery = 75% Analysis Date = 04/19/16 Pct Recovery = 75% Analysis Date = 04/19/16 Pct Recovery = 75% Analysis Date = 04/14/16 Pct Recovery = 75% Analysis Date = 04/14/16 Pct Recovery = 75% Analysis Date = 04/10/16 Pct Recovery = 75% Analysis Date = 04/10/16 Pct Recovery = 75% Analysis Date = 04/05/16 Pct Recovery = 75% Analysis Date = 04/05/16 Pct Recovery = 75% Analysis Date = 03/31/16 Pct Recovery = 75% Analysis Date = 03/31/16 Pct Recovery = 75% Analysis Date = 03/26/16 Pct Recovery = 75% Analysis Date = 03/26/16 Pct Recovery = 75% Analysis Date = 03/21/16 Pct Recovery = 74% Analysis Date = 03/21/16 Pct Recovery = 74% Analysis Date = 03/16/16 Pct Recovery = 74% Analysis Date = 03/16/16 Pct Recovery = 74% Analysis Date = 03/12/16 Pct Recovery = 74% Analysis Date = 03/12/16 Pct Recovery = 74% Analysis Date = 03/07/16 Pct Recovery = 74% Analysis Date = 03/07/16 Pct Recovery = 74% Analysis Date = 03/02/16 Pct Recovery = 74% Analysis Date = 03/02/16 Pct Recovery = 74% Analysis Date = 02/26/16 Pct Recovery = 74% Analysis Date = 02/26/16 Pct Recovery = 74% Analysis Date = 02/21/16 Pct Recovery = 75% Analysis Date = 02/21/16 Pct Recovery = 75% Analysis Date = 02/17/16 Pct Recovery = 75% Analysis Date = 02/17/16 Pct Recovery = 75% Analysis Date = 02/12/16 Pct Recovery = 75% Analysis Date = 02/12/16 Pct Recovery = 75% Analysis Date = 02/07/16 Pct Recovery = 75% Analysis Date = 02/07/16 Pct Recovery = 75% Analysis Date = 02/02/16 Pct Recovery = 75% Analysis Date = 02/02/16 Pct Recovery = 75% Analysis Date = 01/28/16 Pct Recovery = 75% Analysis Date = 01/28/16 Pct Recovery = 75% Analysis Date = 01/23/16 Pct Recovery = 75% Analysis Date = 01/23/16 Pct Recovery = 75% Analysis Date = 01/19/16 Pct Recovery = 75% Analysis Date = 01/19/16 Pct Recovery = 75% Analysis Date = 01/14/16 Pct Recovery = 75% Analysis Date = 01/14/16 Pct Recovery = 75% Analysis Date = 01/09/16 Pct Recovery = 76% Analysis Date = 01/09/16 Pct Recovery = 76% Analysis Date = 01/04/16 Pct Recovery = 76% Analysis Date = 01/04/16 Pct Recovery = 76% Analysis Date = 12/30/15 Pct Recovery = 76% Analysis Date = 12/30/15 Pct Recovery = 76% Analysis Date = 12/26/15 Pct Recovery = 76% Analysis Date = 12/26/15 Pct Recovery = 76% Analysis Date = 12/21/15 Pct Recovery = 76% Analysis Date = 12/21/15 Pct Recovery = 76% Analysis Date = 12/16/15 Pct Recovery = 76% Analysis Date = 12/16/15 Pct Recovery = 76% Analysis Date = 12/11/15 Pct Recovery = 76% Analysis Date = 12/11/15 Pct Recovery = 76% Analysis Date = 12/06/15 Pct Recovery = 76% Analysis Date = 12/06/15 Pct Recovery = 76% Analysis Date = 12/01/15 Pct Recovery = 76% Analysis Date = 12/01/15 Pct Recovery = 76% Analysis Date = 11/27/15 Pct Recovery = 77% Analysis Date = 11/27/15 Pct Recovery = 77% Analysis Date = 11/22/15 Pct Recovery = 77% Analysis Date = 11/22/15 Pct Recovery = 77% Analysis Date = 11/17/15 Pct Recovery = 77% Analysis Date = 11/17/15 Pct Recovery = 77% Analysis Date = 11/12/15 Pct Recovery = 77% Analysis Date = 11/12/15 Pct Recovery = 77% Analysis Date = 11/07/15 Pct Recovery = 77% Analysis Date = 11/07/15 Pct Recovery = 77% Analysis Date = 11/03/15 Pct Recovery = 77% Analysis Date = 11/03/15 Pct Recovery = 77% Analysis Date = 10/29/15 Pct Recovery = 78% Analysis Date = 10/29/15 Pct Recovery = 78% Analysis Date = 10/24/15 Pct Recovery = 78% Analysis Date = 10/24/15 Pct Recovery = 78% Analysis Date = 10/19/15 Pct Recovery = 78% Analysis Date = 10/19/15 Pct Recovery = 78% Analysis Date = 10/14/15 Pct Recovery = 79% Analysis Date = 10/14/15 Pct Recovery = 79% Analysis Date = 10/09/15 Pct Recovery = 79% Analysis Date = 10/09/15 Pct Recovery = 79% Analysis Date = 10/05/15 Pct Recovery = 80% Analysis Date = 10/05/15 Pct Recovery = 80% Analysis Date = 09/30/15 Pct Recovery = 80% Analysis Date = 09/30/15 Pct Recovery = 80% Analysis Date = 09/25/15 Pct Recovery = 80% Analysis Date = 09/25/15 Pct Recovery = 80% Analysis Date = 09/20/15 Pct Recovery = 81% Analysis Date = 09/20/15 Pct Recovery = 81% Analysis Date = 09/15/15 Pct Recovery = 81% Analysis Date = 09/15/15 Pct Recovery = 81% Analysis Date = 09/10/15 Pct Recovery = 81% Analysis Date = 09/10/15 Pct Recovery = 81% Analysis Date = 09/06/15 Pct Recovery = 82% Analysis Date = 09/06/15 Pct Recovery = 82% Analysis Date = 09/01/15 Pct Recovery = 82% Analysis Date = 09/01/15 Pct Recovery = 82% Analysis Date = 08/27/15 Pct Recovery = 83% Analysis Date = 08/27/15 Pct Recovery = 83% Analysis Date = 08/22/15 Pct Recovery = 83% Analysis Date = 08/22/15 Pct Recovery = 83% Analysis Date = 08/17/15 Pct Recovery = 83% Analysis Date = 08/17/15 Pct Recovery = 83% Analysis Date = 08/13/15 Pct Recovery = 84% Analysis Date = 08/13/15 Pct Recovery = 84% Analysis Date = 08/08/15 Pct Recovery = 84% Analysis Date = 08/08/15 Pct Recovery = 84% Analysis Date = 08/03/15 Pct Recovery = 85% Analysis Date = 08/03/15 Pct Recovery = 85% Analysis Date = 07/29/15 Pct Recovery = 85% Analysis Date = 07/29/15 Pct Recovery = 85% Analysis Date = 07/24/15 Pct Recovery = 85% Analysis Date = 07/24/15 Pct Recovery = 85% Analysis Date = 07/19/15 Pct Recovery = 86% Analysis Date = 07/19/15 Pct Recovery = 86% Analysis Date = 07/15/15 Pct Recovery = 86% Analysis Date = 07/15/15 Pct Recovery = 86% Analysis Date = 07/10/15 Pct Recovery = 86% Analysis Date = 07/10/15 Pct Recovery = 86% Analysis Date = 07/05/15 Pct Recovery = 87% Analysis Date = 07/05/15 Pct Recovery = 87% Analysis Date = 06/30/15 Pct Recovery = 87% Analysis Date = 06/30/15 Pct Recovery = 87% Analysis Date = 06/25/15 Pct Recovery = 87% Analysis Date = 06/25/15 Pct Recovery = 87% Analysis Date = 06/21/15 Pct Recovery = 88% Analysis Date = 06/21/15 Pct Recovery = 88% Analysis Date = 06/16/15 Pct Recovery = 88% Analysis Date = 06/16/15 Pct Recovery = 88% Analysis Date = 06/11/15 Pct Recovery = 88% Analysis Date = 06/11/15 Pct Recovery = 88% Analysis Date = 06/06/15 Pct Recovery = 89% Analysis Date = 06/06/15 Pct Recovery = 89% Analysis Date = 06/01/15 Pct Recovery = 89% Analysis Date = 06/01/15 Pct Recovery = 89% Analysis Date = 05/27/15 Pct Recovery = 89% Analysis Date = 05/27/15 Pct Recovery = 89% Analysis Date = 05/23/15 Pct Recovery = 90% Analysis Date = 05/23/15 Pct Recovery = 90% Analysis Date = 05/18/15 Pct Recovery = 90% Analysis Date = 05/18/15 Pct Recovery = 90% Analysis Date = 05/13/15 Pct Recovery = 90% Analysis Date = 05/13/15 Pct Recovery = 90% Analysis Date = 05/08/15 Pct Recovery = 91% Analysis Date = 05/08/15 Pct Recovery = 91% Analysis Date = 05/03/15 Pct Recovery = 91% Analysis Date = 05/03/15 Pct Recovery = 91% Analysis Date = 04/29/15 Pct Recovery = 91% Analysis Date = 04/29/15 Pct Recovery = 91% Analysis Date = 04/24/15 Pct Recovery = 91% Analysis Date = 04/24/15 Pct Recovery = 91% Analysis Date = 04/19/15 Pct Recovery = 91% Analysis Date = 04/19/15 Pct Recovery = 91% Analysis Date = 04/14/15 Pct Recovery = 92% Analysis Date = 04/14/15 Pct Recovery = 92% Analysis Date = 04/09/15 Pct Recovery = 92% Analysis Date = 04/09/15 Pct Recovery = 92% Analysis Date = 04/04/15 Pct Recovery = 92% Analysis Date = 04/04/15 Pct Recovery = 92% Analysis Date = 03/31/15 Pct Recovery = 92% Analysis Date = 03/31/15 Pct Recovery = 92% Analysis Date = 03/26/15 Pct Recovery = 92% Analysis Date = 03/26/15 Pct Recovery = 92% Analysis Date = 03/21/15 Pct Recovery = 92% Analysis Date = 03/21/15 Pct Recovery = 92% Analysis Date = 03/16/15 Pct Recovery = 93% Analysis Date = 03/16/15 Pct Recovery = 93% Analysis Date = 03/11/15 Pct Recovery = 93% Analysis Date = 03/11/15 Pct Recovery = 93% Analysis Date = 03/07/15 Pct Recovery = 93% Analysis Date = 03/07/15 Pct Recovery = 93% Analysis Date = 03/02/15 Pct Recovery = 93% Analysis Date = 03/02/15 Pct Recovery = 93% Analysis Date = 02/25/15 Pct Recovery = 93% Analysis Date = 02/25/15 Pct Recovery = 93% Analysis Date = 02/20/15 Pct Recovery = 93% Analysis Date = 02/20/15 Pct Recovery = 93% Analysis Date = 02/15/15 Pct Recovery = 93% Analysis Date = 02/15/15 Pct Recovery = 93% Analysis Date = 02/10/15 Pct Recovery = 94% Analysis Date = 02/10/15 Pct Recovery = 94% Analysis Date = 02/06/15 Pct Recovery = 94% Analysis Date = 02/06/15 Pct Recovery = 94% Analysis Date = 02/01/15 Pct Recovery = 94% Analysis Date = 02/01/15 Pct Recovery = 94% Analysis Date = 01/27/15 Pct Recovery = 94% Analysis Date = 01/27/15 Pct Recovery = 94% Analysis Date = 01/22/15 Pct Recovery = 94% Analysis Date = 01/22/15 Pct Recovery = 94% Analysis Date = 01/17/15 Pct Recovery = 94% Analysis Date = 01/17/15 Pct Recovery = 94% Analysis Date = 01/12/15 Pct Recovery = 95% Analysis Date = 01/12/15 Pct Recovery = 95% Analysis Date = 01/08/15 Pct Recovery = 95% Analysis Date = 01/08/15 Pct Recovery = 95% Analysis Date = 01/03/15 Pct Recovery = 95% Analysis Date = 01/03/15 Pct Recovery = 95% Analysis Date = 12/29/14 Pct Recovery = 95% Analysis Date = 12/29/14 Pct Recovery = 95% Analysis Date = 12/24/14 Pct Recovery = 95% Analysis Date = 12/24/14 Pct Recovery = 95% Analysis Date = 12/19/14 Pct Recovery = 95% Analysis Date = 12/19/14 Pct Recovery = 95% Analysis Date = 12/15/14 Pct Recovery = 95% Analysis Date = 12/15/14 Pct Recovery = 95% Analysis Date = 12/10/14 Pct Recovery = 96% Analysis Date = 12/10/14 Pct Recovery = 96% Analysis Date = 12/05/14 Pct Recovery = 96% Analysis Date = 12/05/14 Pct Recovery = 96% Analysis Date = 11/30/14 Pct Recovery = 96% Analysis Date = 11/30/14 Pct Recovery = 96% Analysis Date = 11/25/14 Pct Recovery = 96% Analysis Date = 11/25/14 Pct Recovery = 96% Analysis Date = 11/20/14 Pct Recovery = 96% Analysis Date = 11/20/14 Pct Recovery = 96% Analysis Date = 11/16/14 Pct Recovery = 96% Analysis Date = 11/16/14 Pct Recovery = 96% Analysis Date = 11/11/14 Pct Recovery = 96% Analysis Date = 11/11/14 Pct Recovery = 96% Analysis Date = 11/06/14 Pct Recovery = 97% Analysis Date = 11/06/14 Pct Recovery = 97% Analysis Date = 11/01/14 Pct Recovery = 97% Analysis Date = 11/01/14 Pct Recovery = 97% Analysis Date = 10/27/14 Pct Recovery = 97% Analysis Date = 10/27/14 Pct Recovery = 97% Analysis Date = 10/23/14 Pct Recovery = 97% Analysis Date = 10/23/14 Pct Recovery = 97% Analysis Date = 10/18/14 Pct Recovery = 97% Analysis Date = 10/18/14 Pct Recovery = 97% Analysis Date = 10/13/14 Pct Recovery = 97% Analysis Date = 10/13/14 Pct Recovery = 97% Analysis Date = 10/08/14 Pct Recovery = 97% Analysis Date = 10/08/14 Pct Recovery = 97% Analysis Date = 10/03/14 Pct Recovery = 97% Analysis Date = 10/03/14 Pct Recovery = 97% Analysis Date = 09/28/14 Pct Recovery = 98% Analysis Date = 09/28/14 Pct Recovery = 98% Analysis Date = 09/24/14 Pct Recovery = 98% Analysis Date = 09/24/14 Pct Recovery = 98% Analysis Date = 09/19/14 Pct Recovery = 98% Analysis Date = 09/19/14 Pct Recovery = 98% Analysis Date = 09/14/14 Pct Recovery = 98% Analysis Date = 09/14/14 Pct Recovery = 98% Analysis Date = 09/09/14 Pct Recovery = 98% Analysis Date = 09/09/14 Pct Recovery = 98% Analysis Date = 09/04/14 Pct Recovery = 98% Analysis Date = 09/04/14 Pct Recovery = 98% Analysis Date = 08/31/14 Pct Recovery = 98% Analysis Date = 08/31/14 Pct Recovery = 98% Analysis Date = 08/26/14 Pct Recovery = 98% Analysis Date = 08/26/14 Pct Recovery = 98% Analysis Date = 08/21/14 Pct Recovery = 98% Analysis Date = 08/21/14 Pct Recovery = 98% Analysis Date = 08/16/14 Pct Recovery = 98% Analysis Date = 08/16/14 Pct Recovery = 98% Analysis Date = 08/11/14 Pct Recovery = 98% Analysis Date = 08/11/14 Pct Recovery = 98% Analysis Date = 08/06/14 Pct Recovery = 99% Analysis Date = 08/06/14 Pct Recovery = 99% Analysis Date = 08/02/14 Pct Recovery = 99% Analysis Date = 08/02/14 Pct Recovery = 99% Analysis Date = 07/28/14 Pct Recovery = 99% Analysis Date = 07/28/14 Pct Recovery = 99% Analysis Date = 07/23/14 Pct Recovery = 99% Analysis Date = 07/23/14 Pct Recovery = 99% Analysis Date = 07/18/14 Pct Recovery = 99% Analysis Date = 07/18/14 Pct Recovery = 99% Analysis Date = 07/13/14 Pct Recovery = 99% Analysis Date = 07/13/14 Pct Recovery = 99% Analysis Date = 07/09/14 Pct Recovery = 99% Analysis Date = 07/09/14 Pct Recovery = 99% Analysis Date = 07/04/14 Pct Recovery = 99% Analysis Date = 07/04/14 Pct Recovery = 99% Analysis Date = 06/29/14 Pct Recovery = 99% Analysis Date = 06/29/14 Pct Recovery = 99% Analysis Date = 06/24/14 Pct Recovery = 99% Analysis Date = 06/24/14 Pct Recovery = 99% Analysis Date = 06/19/14 Pct Recovery = 99% Analysis Date = 06/19/14 Pct Recovery = 99% Analysis Date = 06/14/14 Pct Recovery = 99% Analysis Date = 06/14/14 Pct Recovery = 99% Analysis Date = 06/10/14 Pct Recovery = 99% Analysis Date = 06/10/14 Pct Recovery = 99% Analysis Date = 06/05/14 Pct Recovery = 99% Analysis Date = 06/05/14 Pct Recovery = 99% Analysis Date = 05/31/14 Pct Recovery = 99% Analysis Date = 05/31/14 Pct Recovery = 99% Analysis Date = 05/26/14 Pct Recovery = 100% Analysis Date = 05/26/14 Pct Recovery = 100% Analysis Date = 05/21/14 Pct Recovery = 100% Analysis Date = 05/21/14 Pct Recovery = 100% Analysis Date = 05/17/14 Pct Recovery = 100% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
BETAMETHASONE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 2 34% 14% 34% 14%
>= Reporting Level 72 87% 18% 87% 19%
Total 74 86% 20% 87% 19%

Sample Statistics
BETAMETHASONE

Characteristic N % % Basis
Plotted 74 99% Spiked
Estimated Values 24 32% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 75 .  
False Negatives 1 1% 1 out of 75
Not Spiked 40 .  
False Positives 0 0% 0 out of 40

BQS OBSP Determination:
BUPROPION
METHOD: 2440 , TESTIDCODE: 67439LCM56
Open Data Set

Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 81% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 79% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 65% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 65% Analysis Date = 01/17/16 SpikeMix = ERA 0406-15-09: 80 µl & ERA 0406-15-07A: 80 µl Pct Recovery = 79% Analysis Date = 11/24/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 89% Analysis Date = 10/01/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 114% Analysis Date = 11/05/15 SpikeMix = ERA 0406-15-08: 80 µl & Abs 052215: 80 µl Pct Recovery = 78% Analysis Date = 11/04/15 SpikeMix = Abs 052215: 80 µl & Abs 050115: 80 µl Pct Recovery = 78% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 70% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 70% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 85% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 84% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 56% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 55% Analysis Date = 09/24/16 SpikeMix = Crescent EN160610015: 80 µl & Abs 061416: 80 µl Pct Recovery = 68% Analysis Date = 09/24/16 SpikeMix = Abs 061416: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 67% Analysis Date = 05/07/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 80% Analysis Date = 03/11/15 SpikeMix = ERA 0318-14-02: 15 µl & Abs 041714: 15 µl Pct Recovery = 83% Analysis Date = 01/16/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 74% Analysis Date = 12/06/14 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 59% Analysis Date = 08/21/14 SpikeMix = ERA 0318-14-02: 60 µl & Abs 041714: 60 µl Pct Recovery = 72% Analysis Date = 07/12/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 74% Analysis Date = 06/11/14 SpikeMix = Abs 041614: 60 µl & Abs 041714: 60 µl Pct Recovery = 83% Analysis Date = 05/21/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 76% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-04: 15 µl & Abs 041814: 15 µl Pct Recovery = 63% Analysis Date = 12/06/14 SpikeMix = ERA 0318-14-02: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 53% Analysis Date = 10/25/14 SpikeMix = Abs 041614: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 67% Analysis Date = 10/11/14 SpikeMix = ERA 0318-14-02: 60 µl & ERA 0319-14-04: 60 µl Pct Recovery = 54% Analysis Date = 08/28/14 SpikeMix = ERA 0319-14-04: 60 µl & ERA 0319-14-05: 60 µl Pct Recovery = 55% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-08: 40 µl & ERA 0406-15-09: 40 µl Pct Recovery = 82% Analysis Date = 07/31/15 SpikeMix = ERA 0406-15-09: 40 µl & Abs 050115: 40 µl Pct Recovery = 93% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-08: 40 µl & Abs 052215: 40 µl Pct Recovery = 69% Analysis Date = 02/23/16 SpikeMix = Abs 052215: 40 µl & Abs 050115: 40 µl Pct Recovery = 80% Analysis Date = 09/10/15 SpikeMix = Abs 052215: 40 µl & ERA 0406-15-07A: 40 µl Pct Recovery = 82% Analysis Date = 07/31/15 SpikeMix = Abs 051315: 40 µl & Abs 052215: 40 µl Pct Recovery = 69% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 69% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 70% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 75% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 74% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 58% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 59% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 68% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 67% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 52% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 57% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 64% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 67% Analysis Date = 11/04/14 SpikeMix = Abs 041714: 8 µl & ERA 0319-14-05: 8 µl Pct Recovery = 65% Analysis Date = 04/30/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 61% Analysis Date = 04/10/15 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 54% Analysis Date = 02/10/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 72% Analysis Date = 12/07/14 SpikeMix = ERA 0318-14-02: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 58% Analysis Date = 10/11/14 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 52% Analysis Date = 10/10/14 SpikeMix = Abs 041714: 30 µl & Abs 041814: 30 µl Pct Recovery = 65% Analysis Date = 07/20/14 SpikeMix = ERA 0318-14-02: 30 µl & Abs 041714: 30 µl Pct Recovery = 60% Analysis Date = 06/28/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 69% Analysis Date = 05/17/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 78% Analysis Date = 09/12/14 SpikeMix = Abs 041614: 30 µl & ERA 0319-14-04: 30 µl Pct Recovery = 43% Analysis Date = 08/16/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 54% Analysis Date = 07/13/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 64% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 82% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 73% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-08: 20 µl & ERA 0406-15-09: 20 µl Pct Recovery = 74% Analysis Date = 11/24/15 SpikeMix = ERA 0406-15-09: 20 µl & Abs 050115: 20 µl Pct Recovery = 87% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-09: 20 µl Pct Recovery = 94% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 37% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 34% Analysis Date = 02/23/16 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 73% Analysis Date = 11/24/15 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 79% Analysis Date = 09/09/15 SpikeMix = ERA 0406-15-08: 20 µl & Abs 052215: 20 µl Pct Recovery = 83% Analysis Date = 08/27/15 SpikeMix = Abs 052215: 20 µl & Abs 050115: 20 µl Pct Recovery = 83% Analysis Date = 07/09/15 SpikeMix = Abs 050115: 20 µl & Abs 052215: 20 µl Pct Recovery = 65% Analysis Date = 06/26/15 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 70% Analysis Date = 04/09/16 SpikeMix = Abs 051315: 10 µl & ERA 0406-15-09: 10 µl Pct Recovery = 71% Analysis Date = 04/09/16 SpikeMix = Abs 051315: 10 µl & ERA 0406-15-09: 10 µl Pct Recovery = 78% Analysis Date = 01/18/17 Pct Recovery = 65% Analysis Date = 01/14/17 Pct Recovery = 65% Analysis Date = 01/14/17 Pct Recovery = 65% Analysis Date = 01/09/17 Pct Recovery = 65% Analysis Date = 01/09/17 Pct Recovery = 65% Analysis Date = 01/04/17 Pct Recovery = 65% Analysis Date = 01/04/17 Pct Recovery = 65% Analysis Date = 12/30/16 Pct Recovery = 66% Analysis Date = 12/30/16 Pct Recovery = 66% Analysis Date = 12/25/16 Pct Recovery = 66% Analysis Date = 12/25/16 Pct Recovery = 66% Analysis Date = 12/20/16 Pct Recovery = 66% Analysis Date = 12/20/16 Pct Recovery = 66% Analysis Date = 12/15/16 Pct Recovery = 66% Analysis Date = 12/15/16 Pct Recovery = 66% Analysis Date = 12/10/16 Pct Recovery = 66% Analysis Date = 12/10/16 Pct Recovery = 66% Analysis Date = 12/05/16 Pct Recovery = 66% Analysis Date = 12/05/16 Pct Recovery = 66% Analysis Date = 12/01/16 Pct Recovery = 66% Analysis Date = 12/01/16 Pct Recovery = 66% Analysis Date = 11/26/16 Pct Recovery = 66% Analysis Date = 11/26/16 Pct Recovery = 66% Analysis Date = 11/21/16 Pct Recovery = 66% Analysis Date = 11/21/16 Pct Recovery = 66% Analysis Date = 11/16/16 Pct Recovery = 66% Analysis Date = 11/16/16 Pct Recovery = 66% Analysis Date = 11/11/16 Pct Recovery = 66% Analysis Date = 11/11/16 Pct Recovery = 66% Analysis Date = 11/06/16 Pct Recovery = 66% Analysis Date = 11/06/16 Pct Recovery = 66% Analysis Date = 11/01/16 Pct Recovery = 66% Analysis Date = 11/01/16 Pct Recovery = 66% Analysis Date = 10/27/16 Pct Recovery = 66% Analysis Date = 10/27/16 Pct Recovery = 66% Analysis Date = 10/22/16 Pct Recovery = 66% Analysis Date = 10/22/16 Pct Recovery = 66% Analysis Date = 10/18/16 Pct Recovery = 66% Analysis Date = 10/18/16 Pct Recovery = 66% Analysis Date = 10/13/16 Pct Recovery = 66% Analysis Date = 10/13/16 Pct Recovery = 66% Analysis Date = 10/08/16 Pct Recovery = 67% Analysis Date = 10/08/16 Pct Recovery = 67% Analysis Date = 10/03/16 Pct Recovery = 67% Analysis Date = 10/03/16 Pct Recovery = 67% Analysis Date = 09/28/16 Pct Recovery = 67% Analysis Date = 09/28/16 Pct Recovery = 67% Analysis Date = 09/23/16 Pct Recovery = 67% Analysis Date = 09/23/16 Pct Recovery = 67% Analysis Date = 09/18/16 Pct Recovery = 67% Analysis Date = 09/18/16 Pct Recovery = 67% Analysis Date = 09/13/16 Pct Recovery = 67% Analysis Date = 09/13/16 Pct Recovery = 67% Analysis Date = 09/08/16 Pct Recovery = 67% Analysis Date = 09/08/16 Pct Recovery = 67% Analysis Date = 09/04/16 Pct Recovery = 67% Analysis Date = 09/04/16 Pct Recovery = 67% Analysis Date = 08/30/16 Pct Recovery = 67% Analysis Date = 08/30/16 Pct Recovery = 67% Analysis Date = 08/25/16 Pct Recovery = 67% Analysis Date = 08/25/16 Pct Recovery = 67% Analysis Date = 08/20/16 Pct Recovery = 67% Analysis Date = 08/20/16 Pct Recovery = 67% Analysis Date = 08/15/16 Pct Recovery = 67% Analysis Date = 08/15/16 Pct Recovery = 67% Analysis Date = 08/10/16 Pct Recovery = 68% Analysis Date = 08/10/16 Pct Recovery = 68% Analysis Date = 08/05/16 Pct Recovery = 68% Analysis Date = 08/05/16 Pct Recovery = 68% Analysis Date = 07/31/16 Pct Recovery = 68% Analysis Date = 07/31/16 Pct Recovery = 68% Analysis Date = 07/26/16 Pct Recovery = 68% Analysis Date = 07/26/16 Pct Recovery = 68% Analysis Date = 07/22/16 Pct Recovery = 68% Analysis Date = 07/22/16 Pct Recovery = 68% Analysis Date = 07/17/16 Pct Recovery = 68% Analysis Date = 07/17/16 Pct Recovery = 68% Analysis Date = 07/12/16 Pct Recovery = 69% Analysis Date = 07/12/16 Pct Recovery = 69% Analysis Date = 07/07/16 Pct Recovery = 69% Analysis Date = 07/07/16 Pct Recovery = 69% Analysis Date = 07/02/16 Pct Recovery = 69% Analysis Date = 07/02/16 Pct Recovery = 69% Analysis Date = 06/27/16 Pct Recovery = 69% Analysis Date = 06/27/16 Pct Recovery = 69% Analysis Date = 06/22/16 Pct Recovery = 69% Analysis Date = 06/22/16 Pct Recovery = 69% Analysis Date = 06/17/16 Pct Recovery = 70% Analysis Date = 06/17/16 Pct Recovery = 70% Analysis Date = 06/12/16 Pct Recovery = 70% Analysis Date = 06/12/16 Pct Recovery = 70% Analysis Date = 06/08/16 Pct Recovery = 70% Analysis Date = 06/08/16 Pct Recovery = 70% Analysis Date = 06/03/16 Pct Recovery = 70% Analysis Date = 06/03/16 Pct Recovery = 70% Analysis Date = 05/29/16 Pct Recovery = 70% Analysis Date = 05/29/16 Pct Recovery = 70% Analysis Date = 05/24/16 Pct Recovery = 70% Analysis Date = 05/24/16 Pct Recovery = 70% Analysis Date = 05/19/16 Pct Recovery = 71% Analysis Date = 05/19/16 Pct Recovery = 71% Analysis Date = 05/14/16 Pct Recovery = 71% Analysis Date = 05/14/16 Pct Recovery = 71% Analysis Date = 05/09/16 Pct Recovery = 71% Analysis Date = 05/09/16 Pct Recovery = 71% Analysis Date = 05/04/16 Pct Recovery = 71% Analysis Date = 05/04/16 Pct Recovery = 71% Analysis Date = 04/29/16 Pct Recovery = 71% Analysis Date = 04/29/16 Pct Recovery = 71% Analysis Date = 04/25/16 Pct Recovery = 72% Analysis Date = 04/25/16 Pct Recovery = 72% Analysis Date = 04/20/16 Pct Recovery = 72% Analysis Date = 04/20/16 Pct Recovery = 72% Analysis Date = 04/15/16 Pct Recovery = 72% Analysis Date = 04/15/16 Pct Recovery = 72% Analysis Date = 04/10/16 Pct Recovery = 72% Analysis Date = 04/10/16 Pct Recovery = 72% Analysis Date = 04/05/16 Pct Recovery = 72% Analysis Date = 04/05/16 Pct Recovery = 72% Analysis Date = 03/31/16 Pct Recovery = 73% Analysis Date = 03/31/16 Pct Recovery = 73% Analysis Date = 03/26/16 Pct Recovery = 73% Analysis Date = 03/26/16 Pct Recovery = 73% Analysis Date = 03/21/16 Pct Recovery = 73% Analysis Date = 03/21/16 Pct Recovery = 73% Analysis Date = 03/16/16 Pct Recovery = 73% Analysis Date = 03/16/16 Pct Recovery = 73% Analysis Date = 03/12/16 Pct Recovery = 74% Analysis Date = 03/12/16 Pct Recovery = 74% Analysis Date = 03/07/16 Pct Recovery = 74% Analysis Date = 03/07/16 Pct Recovery = 74% Analysis Date = 03/02/16 Pct Recovery = 74% Analysis Date = 03/02/16 Pct Recovery = 74% Analysis Date = 02/26/16 Pct Recovery = 74% Analysis Date = 02/26/16 Pct Recovery = 74% Analysis Date = 02/21/16 Pct Recovery = 75% Analysis Date = 02/21/16 Pct Recovery = 75% Analysis Date = 02/16/16 Pct Recovery = 75% Analysis Date = 02/16/16 Pct Recovery = 75% Analysis Date = 02/11/16 Pct Recovery = 75% Analysis Date = 02/11/16 Pct Recovery = 75% Analysis Date = 02/06/16 Pct Recovery = 75% Analysis Date = 02/06/16 Pct Recovery = 75% Analysis Date = 02/01/16 Pct Recovery = 76% Analysis Date = 02/01/16 Pct Recovery = 76% Analysis Date = 01/28/16 Pct Recovery = 76% Analysis Date = 01/28/16 Pct Recovery = 76% Analysis Date = 01/23/16 Pct Recovery = 76% Analysis Date = 01/23/16 Pct Recovery = 76% Analysis Date = 01/18/16 Pct Recovery = 76% Analysis Date = 01/18/16 Pct Recovery = 76% Analysis Date = 01/13/16 Pct Recovery = 76% Analysis Date = 01/13/16 Pct Recovery = 76% Analysis Date = 01/08/16 Pct Recovery = 76% Analysis Date = 01/08/16 Pct Recovery = 76% Analysis Date = 01/03/16 Pct Recovery = 77% Analysis Date = 01/03/16 Pct Recovery = 77% Analysis Date = 12/29/15 Pct Recovery = 77% Analysis Date = 12/29/15 Pct Recovery = 77% Analysis Date = 12/24/15 Pct Recovery = 77% Analysis Date = 12/24/15 Pct Recovery = 77% Analysis Date = 12/19/15 Pct Recovery = 77% Analysis Date = 12/19/15 Pct Recovery = 77% Analysis Date = 12/15/15 Pct Recovery = 77% Analysis Date = 12/15/15 Pct Recovery = 77% Analysis Date = 12/10/15 Pct Recovery = 77% Analysis Date = 12/10/15 Pct Recovery = 77% Analysis Date = 12/05/15 Pct Recovery = 77% Analysis Date = 12/05/15 Pct Recovery = 77% Analysis Date = 11/30/15 Pct Recovery = 77% Analysis Date = 11/30/15 Pct Recovery = 77% Analysis Date = 11/25/15 Pct Recovery = 77% Analysis Date = 11/25/15 Pct Recovery = 77% Analysis Date = 11/20/15 Pct Recovery = 78% Analysis Date = 11/20/15 Pct Recovery = 78% Analysis Date = 11/15/15 Pct Recovery = 78% Analysis Date = 11/15/15 Pct Recovery = 78% Analysis Date = 11/10/15 Pct Recovery = 78% Analysis Date = 11/10/15 Pct Recovery = 78% Analysis Date = 11/05/15 Pct Recovery = 78% Analysis Date = 11/05/15 Pct Recovery = 78% Analysis Date = 11/01/15 Pct Recovery = 78% Analysis Date = 11/01/15 Pct Recovery = 78% Analysis Date = 10/27/15 Pct Recovery = 78% Analysis Date = 10/27/15 Pct Recovery = 78% Analysis Date = 10/22/15 Pct Recovery = 78% Analysis Date = 10/22/15 Pct Recovery = 78% Analysis Date = 10/17/15 Pct Recovery = 78% Analysis Date = 10/17/15 Pct Recovery = 78% Analysis Date = 10/12/15 Pct Recovery = 78% Analysis Date = 10/12/15 Pct Recovery = 78% Analysis Date = 10/07/15 Pct Recovery = 77% Analysis Date = 10/07/15 Pct Recovery = 77% Analysis Date = 10/02/15 Pct Recovery = 77% Analysis Date = 10/02/15 Pct Recovery = 77% Analysis Date = 09/27/15 Pct Recovery = 77% Analysis Date = 09/27/15 Pct Recovery = 77% Analysis Date = 09/22/15 Pct Recovery = 77% Analysis Date = 09/22/15 Pct Recovery = 77% Analysis Date = 09/17/15 Pct Recovery = 77% Analysis Date = 09/17/15 Pct Recovery = 77% Analysis Date = 09/13/15 Pct Recovery = 77% Analysis Date = 09/13/15 Pct Recovery = 77% Analysis Date = 09/08/15 Pct Recovery = 77% Analysis Date = 09/08/15 Pct Recovery = 77% Analysis Date = 09/03/15 Pct Recovery = 77% Analysis Date = 09/03/15 Pct Recovery = 77% Analysis Date = 08/29/15 Pct Recovery = 77% Analysis Date = 08/29/15 Pct Recovery = 77% Analysis Date = 08/24/15 Pct Recovery = 77% Analysis Date = 08/24/15 Pct Recovery = 77% Analysis Date = 08/19/15 Pct Recovery = 77% Analysis Date = 08/19/15 Pct Recovery = 77% Analysis Date = 08/14/15 Pct Recovery = 77% Analysis Date = 08/14/15 Pct Recovery = 77% Analysis Date = 08/09/15 Pct Recovery = 77% Analysis Date = 08/09/15 Pct Recovery = 77% Analysis Date = 08/04/15 Pct Recovery = 76% Analysis Date = 08/04/15 Pct Recovery = 76% Analysis Date = 07/31/15 Pct Recovery = 76% Analysis Date = 07/31/15 Pct Recovery = 76% Analysis Date = 07/26/15 Pct Recovery = 76% Analysis Date = 07/26/15 Pct Recovery = 76% Analysis Date = 07/21/15 Pct Recovery = 76% Analysis Date = 07/21/15 Pct Recovery = 76% Analysis Date = 07/16/15 Pct Recovery = 76% Analysis Date = 07/16/15 Pct Recovery = 76% Analysis Date = 07/11/15 Pct Recovery = 75% Analysis Date = 07/11/15 Pct Recovery = 75% Analysis Date = 07/06/15 Pct Recovery = 75% Analysis Date = 07/06/15 Pct Recovery = 75% Analysis Date = 07/01/15 Pct Recovery = 75% Analysis Date = 07/01/15 Pct Recovery = 75% Analysis Date = 06/26/15 Pct Recovery = 75% Analysis Date = 06/26/15 Pct Recovery = 75% Analysis Date = 06/21/15 Pct Recovery = 75% Analysis Date = 06/21/15 Pct Recovery = 75% Analysis Date = 06/17/15 Pct Recovery = 74% Analysis Date = 06/17/15 Pct Recovery = 74% Analysis Date = 06/12/15 Pct Recovery = 74% Analysis Date = 06/12/15 Pct Recovery = 74% Analysis Date = 06/07/15 Pct Recovery = 74% Analysis Date = 06/07/15 Pct Recovery = 74% Analysis Date = 06/02/15 Pct Recovery = 74% Analysis Date = 06/02/15 Pct Recovery = 74% Analysis Date = 05/28/15 Pct Recovery = 73% Analysis Date = 05/28/15 Pct Recovery = 73% Analysis Date = 05/23/15 Pct Recovery = 73% Analysis Date = 05/23/15 Pct Recovery = 73% Analysis Date = 05/18/15 Pct Recovery = 73% Analysis Date = 05/18/15 Pct Recovery = 73% Analysis Date = 05/13/15 Pct Recovery = 73% Analysis Date = 05/13/15 Pct Recovery = 73% Analysis Date = 05/08/15 Pct Recovery = 72% Analysis Date = 05/08/15 Pct Recovery = 72% Analysis Date = 05/04/15 Pct Recovery = 72% Analysis Date = 05/04/15 Pct Recovery = 72% Analysis Date = 04/29/15 Pct Recovery = 72% Analysis Date = 04/29/15 Pct Recovery = 72% Analysis Date = 04/24/15 Pct Recovery = 72% Analysis Date = 04/24/15 Pct Recovery = 72% Analysis Date = 04/19/15 Pct Recovery = 71% Analysis Date = 04/19/15 Pct Recovery = 71% Analysis Date = 04/14/15 Pct Recovery = 71% Analysis Date = 04/14/15 Pct Recovery = 71% Analysis Date = 04/09/15 Pct Recovery = 71% Analysis Date = 04/09/15 Pct Recovery = 71% Analysis Date = 04/04/15 Pct Recovery = 71% Analysis Date = 04/04/15 Pct Recovery = 71% Analysis Date = 03/30/15 Pct Recovery = 71% Analysis Date = 03/30/15 Pct Recovery = 71% Analysis Date = 03/25/15 Pct Recovery = 71% Analysis Date = 03/25/15 Pct Recovery = 71% Analysis Date = 03/21/15 Pct Recovery = 70% Analysis Date = 03/21/15 Pct Recovery = 70% Analysis Date = 03/16/15 Pct Recovery = 70% Analysis Date = 03/16/15 Pct Recovery = 70% Analysis Date = 03/11/15 Pct Recovery = 70% Analysis Date = 03/11/15 Pct Recovery = 70% Analysis Date = 03/06/15 Pct Recovery = 70% Analysis Date = 03/06/15 Pct Recovery = 70% Analysis Date = 03/01/15 Pct Recovery = 70% Analysis Date = 03/01/15 Pct Recovery = 70% Analysis Date = 02/24/15 Pct Recovery = 70% Analysis Date = 02/24/15 Pct Recovery = 70% Analysis Date = 02/19/15 Pct Recovery = 69% Analysis Date = 02/19/15 Pct Recovery = 69% Analysis Date = 02/14/15 Pct Recovery = 69% Analysis Date = 02/14/15 Pct Recovery = 69% Analysis Date = 02/09/15 Pct Recovery = 69% Analysis Date = 02/09/15 Pct Recovery = 69% Analysis Date = 02/05/15 Pct Recovery = 69% Analysis Date = 02/05/15 Pct Recovery = 69% Analysis Date = 01/31/15 Pct Recovery = 69% Analysis Date = 01/31/15 Pct Recovery = 69% Analysis Date = 01/26/15 Pct Recovery = 69% Analysis Date = 01/26/15 Pct Recovery = 69% Analysis Date = 01/21/15 Pct Recovery = 68% Analysis Date = 01/21/15 Pct Recovery = 68% Analysis Date = 01/16/15 Pct Recovery = 68% Analysis Date = 01/16/15 Pct Recovery = 68% Analysis Date = 01/11/15 Pct Recovery = 68% Analysis Date = 01/11/15 Pct Recovery = 68% Analysis Date = 01/06/15 Pct Recovery = 68% Analysis Date = 01/06/15 Pct Recovery = 68% Analysis Date = 01/01/15 Pct Recovery = 68% Analysis Date = 01/01/15 Pct Recovery = 68% Analysis Date = 12/27/14 Pct Recovery = 68% Analysis Date = 12/27/14 Pct Recovery = 68% Analysis Date = 12/23/14 Pct Recovery = 68% Analysis Date = 12/23/14 Pct Recovery = 68% Analysis Date = 12/18/14 Pct Recovery = 67% Analysis Date = 12/18/14 Pct Recovery = 67% Analysis Date = 12/13/14 Pct Recovery = 67% Analysis Date = 12/13/14 Pct Recovery = 67% Analysis Date = 12/08/14 Pct Recovery = 67% Analysis Date = 12/08/14 Pct Recovery = 67% Analysis Date = 12/03/14 Pct Recovery = 67% Analysis Date = 12/03/14 Pct Recovery = 67% Analysis Date = 11/28/14 Pct Recovery = 67% Analysis Date = 11/28/14 Pct Recovery = 67% Analysis Date = 11/23/14 Pct Recovery = 67% Analysis Date = 11/23/14 Pct Recovery = 67% Analysis Date = 11/18/14 Pct Recovery = 67% Analysis Date = 11/18/14 Pct Recovery = 67% Analysis Date = 11/13/14 Pct Recovery = 66% Analysis Date = 11/13/14 Pct Recovery = 66% Analysis Date = 11/09/14 Pct Recovery = 66% Analysis Date = 11/09/14 Pct Recovery = 66% Analysis Date = 11/04/14 Pct Recovery = 66% Analysis Date = 11/04/14 Pct Recovery = 66% Analysis Date = 10/30/14 Pct Recovery = 66% Analysis Date = 10/30/14 Pct Recovery = 66% Analysis Date = 10/25/14 Pct Recovery = 66% Analysis Date = 10/25/14 Pct Recovery = 66% Analysis Date = 10/20/14 Pct Recovery = 66% Analysis Date = 10/20/14 Pct Recovery = 66% Analysis Date = 10/15/14 Pct Recovery = 66% Analysis Date = 10/15/14 Pct Recovery = 66% Analysis Date = 10/10/14 Pct Recovery = 66% Analysis Date = 10/10/14 Pct Recovery = 66% Analysis Date = 10/05/14 Pct Recovery = 66% Analysis Date = 10/05/14 Pct Recovery = 66% Analysis Date = 09/30/14 Pct Recovery = 65% Analysis Date = 09/30/14 Pct Recovery = 65% Analysis Date = 09/26/14 Pct Recovery = 65% Analysis Date = 09/26/14 Pct Recovery = 65% Analysis Date = 09/21/14 Pct Recovery = 65% Analysis Date = 09/21/14 Pct Recovery = 65% Analysis Date = 09/16/14 Pct Recovery = 65% Analysis Date = 09/16/14 Pct Recovery = 65% Analysis Date = 09/11/14 Pct Recovery = 65% Analysis Date = 09/11/14 Pct Recovery = 65% Analysis Date = 09/06/14 Pct Recovery = 65% Analysis Date = 09/06/14 Pct Recovery = 65% Analysis Date = 09/01/14 Pct Recovery = 65% Analysis Date = 09/01/14 Pct Recovery = 65% Analysis Date = 08/27/14 Pct Recovery = 65% Analysis Date = 08/27/14 Pct Recovery = 65% Analysis Date = 08/22/14 Pct Recovery = 64% Analysis Date = 08/22/14 Pct Recovery = 64% Analysis Date = 08/17/14 Pct Recovery = 64% Analysis Date = 08/17/14 Pct Recovery = 64% Analysis Date = 08/13/14 Pct Recovery = 64% Analysis Date = 08/13/14 Pct Recovery = 64% Analysis Date = 08/08/14 Pct Recovery = 64% Analysis Date = 08/08/14 Pct Recovery = 64% Analysis Date = 08/03/14 Pct Recovery = 64% Analysis Date = 08/03/14 Pct Recovery = 64% Analysis Date = 07/29/14 Pct Recovery = 64% Analysis Date = 07/29/14 Pct Recovery = 64% Analysis Date = 07/24/14 Pct Recovery = 64% Analysis Date = 07/24/14 Pct Recovery = 64% Analysis Date = 07/19/14 Pct Recovery = 64% Analysis Date = 07/19/14 Pct Recovery = 64% Analysis Date = 07/14/14 Pct Recovery = 64% Analysis Date = 07/14/14 Pct Recovery = 64% Analysis Date = 07/09/14 Pct Recovery = 64% Analysis Date = 07/09/14 Pct Recovery = 64% Analysis Date = 07/04/14 Pct Recovery = 63% Analysis Date = 07/04/14 Pct Recovery = 63% Analysis Date = 06/30/14 Pct Recovery = 63% Analysis Date = 06/30/14 Pct Recovery = 63% Analysis Date = 06/25/14 Pct Recovery = 63% Analysis Date = 06/25/14 Pct Recovery = 63% Analysis Date = 06/20/14 Pct Recovery = 63% Analysis Date = 06/20/14 Pct Recovery = 63% Analysis Date = 06/15/14 Pct Recovery = 63% Analysis Date = 06/15/14 Pct Recovery = 63% Analysis Date = 06/10/14 Pct Recovery = 63% Analysis Date = 06/10/14 Pct Recovery = 63% Analysis Date = 06/05/14 Pct Recovery = 63% Analysis Date = 06/05/14 Pct Recovery = 63% Analysis Date = 05/31/14 Pct Recovery = 63% Analysis Date = 05/31/14 Pct Recovery = 63% Analysis Date = 05/26/14 Pct Recovery = 63% Analysis Date = 05/26/14 Pct Recovery = 63% Analysis Date = 05/21/14 Pct Recovery = 63% Analysis Date = 05/21/14 Pct Recovery = 63% Analysis Date = 05/17/14 Pct Recovery = 63% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
BUPROPION

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 2 74% 5% 74% 5%
>= Reporting Level 74 70% 13% 69% 13%
Total 76 70% 13% 70% 12%

Sample Statistics
BUPROPION

Characteristic N % % Basis
Plotted 76 100% Spiked
Estimated Values 1 1% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 76 .  
False Negatives 0 0% 0 out of 76
Not Spiked 39 .  
False Positives 0 0% 0 out of 39

BQS OBSP Determination:
CAFFEINE
METHOD: 2440 , TESTIDCODE: 67440LCM56
Open Data Set

Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 120% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 119% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 96% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 94% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 80 µl & ERA 0406-15-08: 80 µl Pct Recovery = 75% Analysis Date = 11/04/15 SpikeMix = Abs 052215: 80 µl & Abs 050115: 80 µl Pct Recovery = 103% Analysis Date = 01/17/16 SpikeMix = ERA 0406-15-09: 80 µl & ERA 0406-15-07A: 80 µl Pct Recovery = 77% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 80 µl & Abs 051315: 80 µl Pct Recovery = 58% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 97% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 97% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 94% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 91% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 76% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 80% Analysis Date = 09/24/16 SpikeMix = Crescent EN160610015: 80 µl & Abs 061416: 80 µl Pct Recovery = 69% Analysis Date = 09/24/16 SpikeMix = Abs 061416: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 67% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-04: 15 µl & Abs 041814: 15 µl Pct Recovery = 79% Analysis Date = 02/06/15 SpikeMix = Abs 041814: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 76% Analysis Date = 07/12/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 76% Analysis Date = 06/22/14 SpikeMix = Abs 041814: 60 µl & Abs 041614: 60 µl Pct Recovery = 90% Analysis Date = 05/21/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 75% Analysis Date = 05/07/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 87% Analysis Date = 04/29/15 SpikeMix = ERA 0319-14-05: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 124% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 100% Analysis Date = 01/16/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 79% Analysis Date = 12/07/14 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 76% Analysis Date = 12/06/14 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 70% Analysis Date = 08/28/14 SpikeMix = ERA 0319-14-04: 60 µl & ERA 0319-14-05: 60 µl Pct Recovery = 45% Analysis Date = 07/26/14 SpikeMix = ERA 0319-14-05: 60 µl & ERA 0318-14-02: 60 µl Pct Recovery = 86% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 66% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 60% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 84% Analysis Date = 02/23/16 SpikeMix = Abs 052215: 40 µl & Abs 050115: 40 µl Pct Recovery = 86% Analysis Date = 07/31/15 SpikeMix = ERA 0406-15-09: 40 µl & Abs 050115: 40 µl Pct Recovery = 103% Analysis Date = 07/30/15 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 94% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-07A: 40 µl & Abs 051315: 40 µl Pct Recovery = 73% Analysis Date = 11/04/15 SpikeMix = ERA 0406-15-07A: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 88% Analysis Date = 09/10/15 SpikeMix = Abs 052215: 40 µl & ERA 0406-15-07A: 40 µl Pct Recovery = 82% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 81% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 84% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 86% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 81% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 82% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 74% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 82% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 77% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 81% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 78% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 72% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 73% Analysis Date = 04/10/15 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 73% Analysis Date = 11/04/14 SpikeMix = Abs 041814: 8 µl & ERA 0318-14-02: 8 µl Pct Recovery = 84% Analysis Date = 10/11/14 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 144% Analysis Date = 11/04/14 SpikeMix = Abs 041714: 8 µl & ERA 0319-14-05: 8 µl Pct Recovery = 71% Analysis Date = 10/24/14 SpikeMix = ERA 0319-14-05: 8 µl & Abs 041614: 8 µl Pct Recovery = 91% Analysis Date = 10/10/14 SpikeMix = Abs 041714: 30 µl & Abs 041814: 30 µl Pct Recovery = 78% Analysis Date = 10/10/14 SpikeMix = Abs 041814: 30 µl & ERA 0318-14-02: 30 µl Pct Recovery = 76% Analysis Date = 07/13/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 64% Analysis Date = 05/30/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 76% Analysis Date = 08/30/14 SpikeMix = ERA 0318-14-02: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 72% Analysis Date = 08/16/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 37% Analysis Date = 07/13/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 86% Analysis Date = 04/23/14 SpikeMix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.2: 20 µl Pct Recovery = 78% Analysis Date = 11/25/15 SpikeMix = Abs 050115: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 94% Analysis Date = 11/24/15 SpikeMix = ERA 0406-15-09: 20 µl & Abs 050115: 20 µl Pct Recovery = 82% Analysis Date = 08/27/15 SpikeMix = Abs 052215: 20 µl & Abs 050115: 20 µl Pct Recovery = 87% Analysis Date = 08/11/15 SpikeMix = Abs 050115: 20 µl & Abs 051315: 20 µl Pct Recovery = 65% Analysis Date = 07/09/15 SpikeMix = Abs 050115: 20 µl & Abs 052215: 20 µl Pct Recovery = 76% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 86% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 64% Analysis Date = 04/27/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 88% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 107% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 133% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 79% Analysis Date = 11/24/15 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 74% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-09: 20 µl Pct Recovery = 26% Analysis Date = 09/15/15 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 88% Analysis Date = 01/18/17 Pct Recovery = 90% Analysis Date = 01/13/17 Pct Recovery = 90% Analysis Date = 01/13/17 Pct Recovery = 90% Analysis Date = 01/08/17 Pct Recovery = 89% Analysis Date = 01/08/17 Pct Recovery = 89% Analysis Date = 01/03/17 Pct Recovery = 89% Analysis Date = 01/03/17 Pct Recovery = 89% Analysis Date = 12/29/16 Pct Recovery = 89% Analysis Date = 12/29/16 Pct Recovery = 89% Analysis Date = 12/24/16 Pct Recovery = 89% Analysis Date = 12/24/16 Pct Recovery = 89% Analysis Date = 12/19/16 Pct Recovery = 89% Analysis Date = 12/19/16 Pct Recovery = 89% Analysis Date = 12/14/16 Pct Recovery = 89% Analysis Date = 12/14/16 Pct Recovery = 89% Analysis Date = 12/09/16 Pct Recovery = 88% Analysis Date = 12/09/16 Pct Recovery = 88% Analysis Date = 12/04/16 Pct Recovery = 88% Analysis Date = 12/04/16 Pct Recovery = 88% Analysis Date = 11/29/16 Pct Recovery = 88% Analysis Date = 11/29/16 Pct Recovery = 88% Analysis Date = 11/24/16 Pct Recovery = 88% Analysis Date = 11/24/16 Pct Recovery = 88% Analysis Date = 11/19/16 Pct Recovery = 88% Analysis Date = 11/19/16 Pct Recovery = 88% Analysis Date = 11/14/16 Pct Recovery = 88% Analysis Date = 11/14/16 Pct Recovery = 88% Analysis Date = 11/09/16 Pct Recovery = 87% Analysis Date = 11/09/16 Pct Recovery = 87% Analysis Date = 11/04/16 Pct Recovery = 87% Analysis Date = 11/04/16 Pct Recovery = 87% Analysis Date = 10/30/16 Pct Recovery = 87% Analysis Date = 10/30/16 Pct Recovery = 87% Analysis Date = 10/25/16 Pct Recovery = 87% Analysis Date = 10/25/16 Pct Recovery = 87% Analysis Date = 10/20/16 Pct Recovery = 87% Analysis Date = 10/20/16 Pct Recovery = 87% Analysis Date = 10/15/16 Pct Recovery = 87% Analysis Date = 10/15/16 Pct Recovery = 87% Analysis Date = 10/10/16 Pct Recovery = 86% Analysis Date = 10/10/16 Pct Recovery = 86% Analysis Date = 10/05/16 Pct Recovery = 86% Analysis Date = 10/05/16 Pct Recovery = 86% Analysis Date = 09/30/16 Pct Recovery = 86% Analysis Date = 09/30/16 Pct Recovery = 86% Analysis Date = 09/25/16 Pct Recovery = 86% Analysis Date = 09/25/16 Pct Recovery = 86% Analysis Date = 09/20/16 Pct Recovery = 86% Analysis Date = 09/20/16 Pct Recovery = 86% Analysis Date = 09/15/16 Pct Recovery = 86% Analysis Date = 09/15/16 Pct Recovery = 86% Analysis Date = 09/10/16 Pct Recovery = 85% Analysis Date = 09/10/16 Pct Recovery = 85% Analysis Date = 09/05/16 Pct Recovery = 85% Analysis Date = 09/05/16 Pct Recovery = 85% Analysis Date = 08/31/16 Pct Recovery = 85% Analysis Date = 08/31/16 Pct Recovery = 85% Analysis Date = 08/26/16 Pct Recovery = 85% Analysis Date = 08/26/16 Pct Recovery = 85% Analysis Date = 08/21/16 Pct Recovery = 85% Analysis Date = 08/21/16 Pct Recovery = 85% Analysis Date = 08/16/16 Pct Recovery = 85% Analysis Date = 08/16/16 Pct Recovery = 85% Analysis Date = 08/11/16 Pct Recovery = 85% Analysis Date = 08/11/16 Pct Recovery = 85% Analysis Date = 08/06/16 Pct Recovery = 85% Analysis Date = 08/06/16 Pct Recovery = 85% Analysis Date = 08/01/16 Pct Recovery = 84% Analysis Date = 08/01/16 Pct Recovery = 84% Analysis Date = 07/27/16 Pct Recovery = 84% Analysis Date = 07/27/16 Pct Recovery = 84% Analysis Date = 07/22/16 Pct Recovery = 84% Analysis Date = 07/22/16 Pct Recovery = 84% Analysis Date = 07/17/16 Pct Recovery = 84% Analysis Date = 07/17/16 Pct Recovery = 84% Analysis Date = 07/12/16 Pct Recovery = 84% Analysis Date = 07/12/16 Pct Recovery = 84% Analysis Date = 07/07/16 Pct Recovery = 84% Analysis Date = 07/07/16 Pct Recovery = 84% Analysis Date = 07/02/16 Pct Recovery = 84% Analysis Date = 07/02/16 Pct Recovery = 84% Analysis Date = 06/27/16 Pct Recovery = 84% Analysis Date = 06/27/16 Pct Recovery = 84% Analysis Date = 06/22/16 Pct Recovery = 84% Analysis Date = 06/22/16 Pct Recovery = 84% Analysis Date = 06/17/16 Pct Recovery = 84% Analysis Date = 06/17/16 Pct Recovery = 84% Analysis Date = 06/12/16 Pct Recovery = 84% Analysis Date = 06/12/16 Pct Recovery = 84% Analysis Date = 06/07/16 Pct Recovery = 84% Analysis Date = 06/07/16 Pct Recovery = 84% Analysis Date = 06/02/16 Pct Recovery = 84% Analysis Date = 06/02/16 Pct Recovery = 84% Analysis Date = 05/28/16 Pct Recovery = 84% Analysis Date = 05/28/16 Pct Recovery = 84% Analysis Date = 05/23/16 Pct Recovery = 84% Analysis Date = 05/23/16 Pct Recovery = 84% Analysis Date = 05/18/16 Pct Recovery = 83% Analysis Date = 05/18/16 Pct Recovery = 83% Analysis Date = 05/13/16 Pct Recovery = 83% Analysis Date = 05/13/16 Pct Recovery = 83% Analysis Date = 05/08/16 Pct Recovery = 83% Analysis Date = 05/08/16 Pct Recovery = 83% Analysis Date = 05/03/16 Pct Recovery = 83% Analysis Date = 05/03/16 Pct Recovery = 83% Analysis Date = 04/28/16 Pct Recovery = 83% Analysis Date = 04/28/16 Pct Recovery = 83% Analysis Date = 04/23/16 Pct Recovery = 83% Analysis Date = 04/23/16 Pct Recovery = 83% Analysis Date = 04/18/16 Pct Recovery = 83% Analysis Date = 04/18/16 Pct Recovery = 83% Analysis Date = 04/13/16 Pct Recovery = 83% Analysis Date = 04/13/16 Pct Recovery = 83% Analysis Date = 04/08/16 Pct Recovery = 83% Analysis Date = 04/08/16 Pct Recovery = 83% Analysis Date = 04/03/16 Pct Recovery = 83% Analysis Date = 04/03/16 Pct Recovery = 83% Analysis Date = 03/29/16 Pct Recovery = 83% Analysis Date = 03/29/16 Pct Recovery = 83% Analysis Date = 03/24/16 Pct Recovery = 83% Analysis Date = 03/24/16 Pct Recovery = 83% Analysis Date = 03/19/16 Pct Recovery = 82% Analysis Date = 03/19/16 Pct Recovery = 82% Analysis Date = 03/14/16 Pct Recovery = 82% Analysis Date = 03/14/16 Pct Recovery = 82% Analysis Date = 03/09/16 Pct Recovery = 82% Analysis Date = 03/09/16 Pct Recovery = 82% Analysis Date = 03/04/16 Pct Recovery = 82% Analysis Date = 03/04/16 Pct Recovery = 82% Analysis Date = 02/28/16 Pct Recovery = 82% Analysis Date = 02/28/16 Pct Recovery = 82% Analysis Date = 02/23/16 Pct Recovery = 82% Analysis Date = 02/23/16 Pct Recovery = 82% Analysis Date = 02/18/16 Pct Recovery = 82% Analysis Date = 02/18/16 Pct Recovery = 82% Analysis Date = 02/13/16 Pct Recovery = 82% Analysis Date = 02/13/16 Pct Recovery = 82% Analysis Date = 02/08/16 Pct Recovery = 82% Analysis Date = 02/08/16 Pct Recovery = 82% Analysis Date = 02/03/16 Pct Recovery = 82% Analysis Date = 02/03/16 Pct Recovery = 82% Analysis Date = 01/29/16 Pct Recovery = 82% Analysis Date = 01/29/16 Pct Recovery = 82% Analysis Date = 01/24/16 Pct Recovery = 82% Analysis Date = 01/24/16 Pct Recovery = 82% Analysis Date = 01/19/16 Pct Recovery = 82% Analysis Date = 01/19/16 Pct Recovery = 82% Analysis Date = 01/14/16 Pct Recovery = 82% Analysis Date = 01/14/16 Pct Recovery = 82% Analysis Date = 01/09/16 Pct Recovery = 82% Analysis Date = 01/09/16 Pct Recovery = 82% Analysis Date = 01/04/16 Pct Recovery = 82% Analysis Date = 01/04/16 Pct Recovery = 82% Analysis Date = 12/30/15 Pct Recovery = 82% Analysis Date = 12/30/15 Pct Recovery = 82% Analysis Date = 12/25/15 Pct Recovery = 82% Analysis Date = 12/25/15 Pct Recovery = 82% Analysis Date = 12/20/15 Pct Recovery = 82% Analysis Date = 12/20/15 Pct Recovery = 82% Analysis Date = 12/15/15 Pct Recovery = 82% Analysis Date = 12/15/15 Pct Recovery = 82% Analysis Date = 12/10/15 Pct Recovery = 82% Analysis Date = 12/10/15 Pct Recovery = 82% Analysis Date = 12/05/15 Pct Recovery = 82% Analysis Date = 12/05/15 Pct Recovery = 82% Analysis Date = 11/30/15 Pct Recovery = 82% Analysis Date = 11/30/15 Pct Recovery = 82% Analysis Date = 11/25/15 Pct Recovery = 82% Analysis Date = 11/25/15 Pct Recovery = 82% Analysis Date = 11/20/15 Pct Recovery = 82% Analysis Date = 11/20/15 Pct Recovery = 82% Analysis Date = 11/15/15 Pct Recovery = 82% Analysis Date = 11/15/15 Pct Recovery = 82% Analysis Date = 11/10/15 Pct Recovery = 82% Analysis Date = 11/10/15 Pct Recovery = 82% Analysis Date = 11/05/15 Pct Recovery = 82% Analysis Date = 11/05/15 Pct Recovery = 82% Analysis Date = 10/31/15 Pct Recovery = 82% Analysis Date = 10/31/15 Pct Recovery = 82% Analysis Date = 10/26/15 Pct Recovery = 82% Analysis Date = 10/26/15 Pct Recovery = 82% Analysis Date = 10/21/15 Pct Recovery = 82% Analysis Date = 10/21/15 Pct Recovery = 82% Analysis Date = 10/16/15 Pct Recovery = 82% Analysis Date = 10/16/15 Pct Recovery = 82% Analysis Date = 10/11/15 Pct Recovery = 82% Analysis Date = 10/11/15 Pct Recovery = 82% Analysis Date = 10/06/15 Pct Recovery = 82% Analysis Date = 10/06/15 Pct Recovery = 82% Analysis Date = 10/01/15 Pct Recovery = 82% Analysis Date = 10/01/15 Pct Recovery = 82% Analysis Date = 09/26/15 Pct Recovery = 82% Analysis Date = 09/26/15 Pct Recovery = 82% Analysis Date = 09/21/15 Pct Recovery = 82% Analysis Date = 09/21/15 Pct Recovery = 82% Analysis Date = 09/16/15 Pct Recovery = 82% Analysis Date = 09/16/15 Pct Recovery = 82% Analysis Date = 09/11/15 Pct Recovery = 82% Analysis Date = 09/11/15 Pct Recovery = 82% Analysis Date = 09/05/15 Pct Recovery = 82% Analysis Date = 09/05/15 Pct Recovery = 82% Analysis Date = 08/31/15 Pct Recovery = 82% Analysis Date = 08/31/15 Pct Recovery = 82% Analysis Date = 08/26/15 Pct Recovery = 82% Analysis Date = 08/26/15 Pct Recovery = 82% Analysis Date = 08/21/15 Pct Recovery = 83% Analysis Date = 08/21/15 Pct Recovery = 83% Analysis Date = 08/16/15 Pct Recovery = 83% Analysis Date = 08/16/15 Pct Recovery = 83% Analysis Date = 08/11/15 Pct Recovery = 83% Analysis Date = 08/11/15 Pct Recovery = 83% Analysis Date = 08/06/15 Pct Recovery = 83% Analysis Date = 08/06/15 Pct Recovery = 83% Analysis Date = 08/01/15 Pct Recovery = 83% Analysis Date = 08/01/15 Pct Recovery = 83% Analysis Date = 07/27/15 Pct Recovery = 83% Analysis Date = 07/27/15 Pct Recovery = 83% Analysis Date = 07/22/15 Pct Recovery = 83% Analysis Date = 07/22/15 Pct Recovery = 83% Analysis Date = 07/17/15 Pct Recovery = 82% Analysis Date = 07/17/15 Pct Recovery = 82% Analysis Date = 07/12/15 Pct Recovery = 82% Analysis Date = 07/12/15 Pct Recovery = 82% Analysis Date = 07/07/15 Pct Recovery = 82% Analysis Date = 07/07/15 Pct Recovery = 82% Analysis Date = 07/02/15 Pct Recovery = 82% Analysis Date = 07/02/15 Pct Recovery = 82% Analysis Date = 06/27/15 Pct Recovery = 82% Analysis Date = 06/27/15 Pct Recovery = 82% Analysis Date = 06/22/15 Pct Recovery = 82% Analysis Date = 06/22/15 Pct Recovery = 82% Analysis Date = 06/17/15 Pct Recovery = 82% Analysis Date = 06/17/15 Pct Recovery = 82% Analysis Date = 06/12/15 Pct Recovery = 82% Analysis Date = 06/12/15 Pct Recovery = 82% Analysis Date = 06/07/15 Pct Recovery = 82% Analysis Date = 06/07/15 Pct Recovery = 82% Analysis Date = 06/02/15 Pct Recovery = 82% Analysis Date = 06/02/15 Pct Recovery = 82% Analysis Date = 05/28/15 Pct Recovery = 82% Analysis Date = 05/28/15 Pct Recovery = 82% Analysis Date = 05/23/15 Pct Recovery = 82% Analysis Date = 05/23/15 Pct Recovery = 82% Analysis Date = 05/18/15 Pct Recovery = 82% Analysis Date = 05/18/15 Pct Recovery = 82% Analysis Date = 05/13/15 Pct Recovery = 82% Analysis Date = 05/13/15 Pct Recovery = 82% Analysis Date = 05/08/15 Pct Recovery = 82% Analysis Date = 05/08/15 Pct Recovery = 82% Analysis Date = 05/03/15 Pct Recovery = 82% Analysis Date = 05/03/15 Pct Recovery = 82% Analysis Date = 04/28/15 Pct Recovery = 82% Analysis Date = 04/28/15 Pct Recovery = 82% Analysis Date = 04/23/15 Pct Recovery = 82% Analysis Date = 04/23/15 Pct Recovery = 82% Analysis Date = 04/18/15 Pct Recovery = 82% Analysis Date = 04/18/15 Pct Recovery = 82% Analysis Date = 04/13/15 Pct Recovery = 82% Analysis Date = 04/13/15 Pct Recovery = 82% Analysis Date = 04/08/15 Pct Recovery = 82% Analysis Date = 04/08/15 Pct Recovery = 82% Analysis Date = 04/03/15 Pct Recovery = 82% Analysis Date = 04/03/15 Pct Recovery = 82% Analysis Date = 03/29/15 Pct Recovery = 82% Analysis Date = 03/29/15 Pct Recovery = 82% Analysis Date = 03/24/15 Pct Recovery = 82% Analysis Date = 03/24/15 Pct Recovery = 82% Analysis Date = 03/19/15 Pct Recovery = 82% Analysis Date = 03/19/15 Pct Recovery = 82% Analysis Date = 03/14/15 Pct Recovery = 82% Analysis Date = 03/14/15 Pct Recovery = 82% Analysis Date = 03/09/15 Pct Recovery = 81% Analysis Date = 03/09/15 Pct Recovery = 81% Analysis Date = 03/04/15 Pct Recovery = 81% Analysis Date = 03/04/15 Pct Recovery = 81% Analysis Date = 02/27/15 Pct Recovery = 81% Analysis Date = 02/27/15 Pct Recovery = 81% Analysis Date = 02/22/15 Pct Recovery = 81% Analysis Date = 02/22/15 Pct Recovery = 81% Analysis Date = 02/17/15 Pct Recovery = 81% Analysis Date = 02/17/15 Pct Recovery = 81% Analysis Date = 02/12/15 Pct Recovery = 81% Analysis Date = 02/12/15 Pct Recovery = 81% Analysis Date = 02/07/15 Pct Recovery = 81% Analysis Date = 02/07/15 Pct Recovery = 81% Analysis Date = 02/02/15 Pct Recovery = 81% Analysis Date = 02/02/15 Pct Recovery = 81% Analysis Date = 01/28/15 Pct Recovery = 81% Analysis Date = 01/28/15 Pct Recovery = 81% Analysis Date = 01/23/15 Pct Recovery = 81% Analysis Date = 01/23/15 Pct Recovery = 81% Analysis Date = 01/18/15 Pct Recovery = 81% Analysis Date = 01/18/15 Pct Recovery = 81% Analysis Date = 01/13/15 Pct Recovery = 81% Analysis Date = 01/13/15 Pct Recovery = 81% Analysis Date = 01/08/15 Pct Recovery = 81% Analysis Date = 01/08/15 Pct Recovery = 81% Analysis Date = 01/03/15 Pct Recovery = 81% Analysis Date = 01/03/15 Pct Recovery = 81% Analysis Date = 12/29/14 Pct Recovery = 80% Analysis Date = 12/29/14 Pct Recovery = 80% Analysis Date = 12/24/14 Pct Recovery = 80% Analysis Date = 12/24/14 Pct Recovery = 80% Analysis Date = 12/19/14 Pct Recovery = 80% Analysis Date = 12/19/14 Pct Recovery = 80% Analysis Date = 12/14/14 Pct Recovery = 80% Analysis Date = 12/14/14 Pct Recovery = 80% Analysis Date = 12/09/14 Pct Recovery = 80% Analysis Date = 12/09/14 Pct Recovery = 80% Analysis Date = 12/04/14 Pct Recovery = 80% Analysis Date = 12/04/14 Pct Recovery = 80% Analysis Date = 11/29/14 Pct Recovery = 80% Analysis Date = 11/29/14 Pct Recovery = 80% Analysis Date = 11/24/14 Pct Recovery = 80% Analysis Date = 11/24/14 Pct Recovery = 80% Analysis Date = 11/19/14 Pct Recovery = 80% Analysis Date = 11/19/14 Pct Recovery = 80% Analysis Date = 11/14/14 Pct Recovery = 80% Analysis Date = 11/14/14 Pct Recovery = 80% Analysis Date = 11/09/14 Pct Recovery = 80% Analysis Date = 11/09/14 Pct Recovery = 80% Analysis Date = 11/04/14 Pct Recovery = 79% Analysis Date = 11/04/14 Pct Recovery = 79% Analysis Date = 10/30/14 Pct Recovery = 79% Analysis Date = 10/30/14 Pct Recovery = 79% Analysis Date = 10/25/14 Pct Recovery = 79% Analysis Date = 10/25/14 Pct Recovery = 79% Analysis Date = 10/20/14 Pct Recovery = 79% Analysis Date = 10/20/14 Pct Recovery = 79% Analysis Date = 10/15/14 Pct Recovery = 79% Analysis Date = 10/15/14 Pct Recovery = 79% Analysis Date = 10/10/14 Pct Recovery = 79% Analysis Date = 10/10/14 Pct Recovery = 79% Analysis Date = 10/05/14 Pct Recovery = 79% Analysis Date = 10/05/14 Pct Recovery = 79% Analysis Date = 09/30/14 Pct Recovery = 79% Analysis Date = 09/30/14 Pct Recovery = 79% Analysis Date = 09/25/14 Pct Recovery = 79% Analysis Date = 09/25/14 Pct Recovery = 79% Analysis Date = 09/20/14 Pct Recovery = 79% Analysis Date = 09/20/14 Pct Recovery = 79% Analysis Date = 09/15/14 Pct Recovery = 78% Analysis Date = 09/15/14 Pct Recovery = 78% Analysis Date = 09/10/14 Pct Recovery = 78% Analysis Date = 09/10/14 Pct Recovery = 78% Analysis Date = 09/05/14 Pct Recovery = 78% Analysis Date = 09/05/14 Pct Recovery = 78% Analysis Date = 08/31/14 Pct Recovery = 78% Analysis Date = 08/31/14 Pct Recovery = 78% Analysis Date = 08/26/14 Pct Recovery = 78% Analysis Date = 08/26/14 Pct Recovery = 78% Analysis Date = 08/21/14 Pct Recovery = 78% Analysis Date = 08/21/14 Pct Recovery = 78% Analysis Date = 08/16/14 Pct Recovery = 78% Analysis Date = 08/16/14 Pct Recovery = 78% Analysis Date = 08/11/14 Pct Recovery = 78% Analysis Date = 08/11/14 Pct Recovery = 78% Analysis Date = 08/06/14 Pct Recovery = 78% Analysis Date = 08/06/14 Pct Recovery = 78% Analysis Date = 08/01/14 Pct Recovery = 77% Analysis Date = 08/01/14 Pct Recovery = 77% Analysis Date = 07/27/14 Pct Recovery = 77% Analysis Date = 07/27/14 Pct Recovery = 77% Analysis Date = 07/22/14 Pct Recovery = 77% Analysis Date = 07/22/14 Pct Recovery = 77% Analysis Date = 07/17/14 Pct Recovery = 77% Analysis Date = 07/17/14 Pct Recovery = 77% Analysis Date = 07/12/14 Pct Recovery = 77% Analysis Date = 07/12/14 Pct Recovery = 77% Analysis Date = 07/07/14 Pct Recovery = 77% Analysis Date = 07/07/14 Pct Recovery = 77% Analysis Date = 07/02/14 Pct Recovery = 77% Analysis Date = 07/02/14 Pct Recovery = 77% Analysis Date = 06/27/14 Pct Recovery = 77% Analysis Date = 06/27/14 Pct Recovery = 77% Analysis Date = 06/22/14 Pct Recovery = 76% Analysis Date = 06/22/14 Pct Recovery = 76% Analysis Date = 06/17/14 Pct Recovery = 76% Analysis Date = 06/17/14 Pct Recovery = 76% Analysis Date = 06/12/14 Pct Recovery = 76% Analysis Date = 06/12/14 Pct Recovery = 76% Analysis Date = 06/07/14 Pct Recovery = 76% Analysis Date = 06/07/14 Pct Recovery = 76% Analysis Date = 06/02/14 Pct Recovery = 76% Analysis Date = 06/02/14 Pct Recovery = 76% Analysis Date = 05/28/14 Pct Recovery = 76% Analysis Date = 05/28/14 Pct Recovery = 76% Analysis Date = 05/23/14 Pct Recovery = 76% Analysis Date = 05/23/14 Pct Recovery = 76% Analysis Date = 05/18/14 Pct Recovery = 76% Analysis Date = 05/18/14 Pct Recovery = 76% Analysis Date = 05/13/14 Pct Recovery = 75% Analysis Date = 05/13/14 Pct Recovery = 75% Analysis Date = 05/08/14 Pct Recovery = 75% Analysis Date = 05/08/14 Pct Recovery = 75% Analysis Date = 05/03/14 Pct Recovery = 75% Analysis Date = 05/03/14 Pct Recovery = 75% Analysis Date = 04/28/14 Pct Recovery = 75% Analysis Date = 04/28/14 Pct Recovery = 75% Analysis Date = 04/23/14 Pct Recovery = 75% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
CAFFEINE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 77 82% 18% 81% 10%
Total 77 82% 18% 81% 10%

Sample Statistics
CAFFEINE

Characteristic N % % Basis
Plotted 77 99% Spiked
Estimated Values 26 33% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 1 1% Spiked
Spiked 78 .  
False Negatives 0 0% 0 out of 78
Not Spiked 37 .  
False Positives 3 8% 3 out of 37

BQS OBSP Determination:
CARBAMAZEPINE
METHOD: 2440 , TESTIDCODE: 67441LCM56
Open Data Set

Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 78% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 84% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 80 µl & ERA 0406-15-08: 80 µl Pct Recovery = 78% Analysis Date = 11/05/15 SpikeMix = ERA 0406-15-08: 80 µl & Abs 052215: 80 µl Pct Recovery = 80% Analysis Date = 11/24/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 82% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 80 µl & Abs 051315: 80 µl Pct Recovery = 76% Analysis Date = 10/01/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 69% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 81% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 82% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 94% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 90% Analysis Date = 11/18/16 SpikeMix = ERA 04281604: 80 µl & ERA 04281603: 80 µl Pct Recovery = 82% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & ERA 04281604: 80 µl Pct Recovery = 83% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 76% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 77% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-08: 40 µl & Abs 052215: 40 µl Pct Recovery = 76% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 84% Analysis Date = 11/04/15 SpikeMix = ERA 0406-15-07A: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 69% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-08: 40 µl & ERA 0406-15-09: 40 µl Pct Recovery = 70% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 78% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 68% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-07A: 40 µl & Abs 051315: 40 µl Pct Recovery = 75% Analysis Date = 07/31/15 SpikeMix = Abs 051315: 40 µl & Abs 052215: 40 µl Pct Recovery = 73% Analysis Date = 07/30/15 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 85% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 102% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 105% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 95% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 86% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 82% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 79% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 69% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 73% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 73% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 59% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 78% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 78% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 63% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 65% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-04: 15 µl & Abs 041814: 15 µl Pct Recovery = 80% Analysis Date = 12/06/14 SpikeMix = ERA 0318-14-02: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 72% Analysis Date = 10/25/14 SpikeMix = Abs 041614: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 77% Analysis Date = 10/11/14 SpikeMix = ERA 0318-14-02: 60 µl & ERA 0319-14-04: 60 µl Pct Recovery = 65% Analysis Date = 08/28/14 SpikeMix = ERA 0319-14-04: 60 µl & ERA 0319-14-05: 60 µl Pct Recovery = 58% Analysis Date = 04/27/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 93% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 74% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-08: 20 µl & ERA 0406-15-09: 20 µl Pct Recovery = 62% Analysis Date = 11/25/15 SpikeMix = Abs 050115: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 80% Analysis Date = 09/15/15 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 89% Analysis Date = 09/09/15 SpikeMix = ERA 0406-15-08: 20 µl & Abs 052215: 20 µl Pct Recovery = 74% Analysis Date = 05/07/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 105% Analysis Date = 03/11/15 SpikeMix = ERA 0318-14-02: 15 µl & Abs 041714: 15 µl Pct Recovery = 89% Analysis Date = 01/16/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 86% Analysis Date = 12/06/14 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 86% Analysis Date = 08/21/14 SpikeMix = ERA 0318-14-02: 60 µl & Abs 041714: 60 µl Pct Recovery = 74% Analysis Date = 07/12/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 76% Analysis Date = 06/11/14 SpikeMix = Abs 041614: 60 µl & Abs 041714: 60 µl Pct Recovery = 82% Analysis Date = 05/21/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 76% Analysis Date = 02/23/16 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 78% Analysis Date = 08/11/15 SpikeMix = Abs 050115: 20 µl & Abs 051315: 20 µl Pct Recovery = 54% Analysis Date = 06/26/15 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 77% Analysis Date = 06/09/15 SpikeMix = Abs 051315: 20 µl & Abs 050115: 20 µl Pct Recovery = 66% Analysis Date = 04/23/14 SpikeMix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.2: 20 µl Pct Recovery = 72% Analysis Date = 04/30/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 47% Analysis Date = 04/10/15 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 60% Analysis Date = 02/10/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 79% Analysis Date = 12/07/14 SpikeMix = ERA 0318-14-02: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 88% Analysis Date = 10/11/14 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 54% Analysis Date = 11/04/14 SpikeMix = Abs 041714: 8 µl & ERA 0319-14-05: 8 µl Pct Recovery = 70% Analysis Date = 09/12/14 SpikeMix = Abs 041614: 30 µl & ERA 0319-14-04: 30 µl Pct Recovery = 63% Analysis Date = 08/16/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 73% Analysis Date = 07/13/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 77% Analysis Date = 10/10/14 SpikeMix = Abs 041714: 30 µl & Abs 041814: 30 µl Pct Recovery = 71% Analysis Date = 07/20/14 SpikeMix = ERA 0318-14-02: 30 µl & Abs 041714: 30 µl Pct Recovery = 71% Analysis Date = 06/28/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 60% Analysis Date = 05/17/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 85% Analysis Date = 04/09/16 SpikeMix = Abs 051315: 10 µl & ERA 0406-15-09: 10 µl Pct Recovery = 90% Analysis Date = 01/18/17 Pct Recovery = 84% Analysis Date = 01/13/17 Pct Recovery = 84% Analysis Date = 01/13/17 Pct Recovery = 84% Analysis Date = 01/08/17 Pct Recovery = 84% Analysis Date = 01/08/17 Pct Recovery = 84% Analysis Date = 01/03/17 Pct Recovery = 84% Analysis Date = 01/03/17 Pct Recovery = 84% Analysis Date = 12/29/16 Pct Recovery = 84% Analysis Date = 12/29/16 Pct Recovery = 84% Analysis Date = 12/24/16 Pct Recovery = 84% Analysis Date = 12/24/16 Pct Recovery = 84% Analysis Date = 12/19/16 Pct Recovery = 83% Analysis Date = 12/19/16 Pct Recovery = 83% Analysis Date = 12/14/16 Pct Recovery = 83% Analysis Date = 12/14/16 Pct Recovery = 83% Analysis Date = 12/09/16 Pct Recovery = 83% Analysis Date = 12/09/16 Pct Recovery = 83% Analysis Date = 12/04/16 Pct Recovery = 83% Analysis Date = 12/04/16 Pct Recovery = 83% Analysis Date = 11/29/16 Pct Recovery = 83% Analysis Date = 11/29/16 Pct Recovery = 83% Analysis Date = 11/24/16 Pct Recovery = 83% Analysis Date = 11/24/16 Pct Recovery = 83% Analysis Date = 11/19/16 Pct Recovery = 83% Analysis Date = 11/19/16 Pct Recovery = 83% Analysis Date = 11/14/16 Pct Recovery = 82% Analysis Date = 11/14/16 Pct Recovery = 82% Analysis Date = 11/09/16 Pct Recovery = 82% Analysis Date = 11/09/16 Pct Recovery = 82% Analysis Date = 11/04/16 Pct Recovery = 82% Analysis Date = 11/04/16 Pct Recovery = 82% Analysis Date = 10/30/16 Pct Recovery = 82% Analysis Date = 10/30/16 Pct Recovery = 82% Analysis Date = 10/25/16 Pct Recovery = 82% Analysis Date = 10/25/16 Pct Recovery = 82% Analysis Date = 10/20/16 Pct Recovery = 82% Analysis Date = 10/20/16 Pct Recovery = 82% Analysis Date = 10/15/16 Pct Recovery = 82% Analysis Date = 10/15/16 Pct Recovery = 82% Analysis Date = 10/10/16 Pct Recovery = 81% Analysis Date = 10/10/16 Pct Recovery = 81% Analysis Date = 10/05/16 Pct Recovery = 81% Analysis Date = 10/05/16 Pct Recovery = 81% Analysis Date = 09/30/16 Pct Recovery = 81% Analysis Date = 09/30/16 Pct Recovery = 81% Analysis Date = 09/25/16 Pct Recovery = 81% Analysis Date = 09/25/16 Pct Recovery = 81% Analysis Date = 09/20/16 Pct Recovery = 81% Analysis Date = 09/20/16 Pct Recovery = 81% Analysis Date = 09/15/16 Pct Recovery = 81% Analysis Date = 09/15/16 Pct Recovery = 81% Analysis Date = 09/10/16 Pct Recovery = 81% Analysis Date = 09/10/16 Pct Recovery = 81% Analysis Date = 09/05/16 Pct Recovery = 81% Analysis Date = 09/05/16 Pct Recovery = 81% Analysis Date = 08/31/16 Pct Recovery = 80% Analysis Date = 08/31/16 Pct Recovery = 80% Analysis Date = 08/26/16 Pct Recovery = 80% Analysis Date = 08/26/16 Pct Recovery = 80% Analysis Date = 08/21/16 Pct Recovery = 80% Analysis Date = 08/21/16 Pct Recovery = 80% Analysis Date = 08/16/16 Pct Recovery = 80% Analysis Date = 08/16/16 Pct Recovery = 80% Analysis Date = 08/11/16 Pct Recovery = 80% Analysis Date = 08/11/16 Pct Recovery = 80% Analysis Date = 08/06/16 Pct Recovery = 80% Analysis Date = 08/06/16 Pct Recovery = 80% Analysis Date = 08/01/16 Pct Recovery = 80% Analysis Date = 08/01/16 Pct Recovery = 80% Analysis Date = 07/27/16 Pct Recovery = 80% Analysis Date = 07/27/16 Pct Recovery = 80% Analysis Date = 07/22/16 Pct Recovery = 80% Analysis Date = 07/22/16 Pct Recovery = 80% Analysis Date = 07/17/16 Pct Recovery = 80% Analysis Date = 07/17/16 Pct Recovery = 80% Analysis Date = 07/12/16 Pct Recovery = 79% Analysis Date = 07/12/16 Pct Recovery = 79% Analysis Date = 07/07/16 Pct Recovery = 79% Analysis Date = 07/07/16 Pct Recovery = 79% Analysis Date = 07/02/16 Pct Recovery = 79% Analysis Date = 07/02/16 Pct Recovery = 79% Analysis Date = 06/27/16 Pct Recovery = 79% Analysis Date = 06/27/16 Pct Recovery = 79% Analysis Date = 06/22/16 Pct Recovery = 79% Analysis Date = 06/22/16 Pct Recovery = 79% Analysis Date = 06/17/16 Pct Recovery = 79% Analysis Date = 06/17/16 Pct Recovery = 79% Analysis Date = 06/12/16 Pct Recovery = 79% Analysis Date = 06/12/16 Pct Recovery = 79% Analysis Date = 06/07/16 Pct Recovery = 79% Analysis Date = 06/07/16 Pct Recovery = 79% Analysis Date = 06/02/16 Pct Recovery = 79% Analysis Date = 06/02/16 Pct Recovery = 79% Analysis Date = 05/28/16 Pct Recovery = 79% Analysis Date = 05/28/16 Pct Recovery = 79% Analysis Date = 05/23/16 Pct Recovery = 78% Analysis Date = 05/23/16 Pct Recovery = 78% Analysis Date = 05/18/16 Pct Recovery = 78% Analysis Date = 05/18/16 Pct Recovery = 78% Analysis Date = 05/13/16 Pct Recovery = 78% Analysis Date = 05/13/16 Pct Recovery = 78% Analysis Date = 05/08/16 Pct Recovery = 78% Analysis Date = 05/08/16 Pct Recovery = 78% Analysis Date = 05/03/16 Pct Recovery = 78% Analysis Date = 05/03/16 Pct Recovery = 78% Analysis Date = 04/28/16 Pct Recovery = 78% Analysis Date = 04/28/16 Pct Recovery = 78% Analysis Date = 04/23/16 Pct Recovery = 78% Analysis Date = 04/23/16 Pct Recovery = 78% Analysis Date = 04/18/16 Pct Recovery = 78% Analysis Date = 04/18/16 Pct Recovery = 78% Analysis Date = 04/13/16 Pct Recovery = 78% Analysis Date = 04/13/16 Pct Recovery = 78% Analysis Date = 04/08/16 Pct Recovery = 78% Analysis Date = 04/08/16 Pct Recovery = 78% Analysis Date = 04/03/16 Pct Recovery = 78% Analysis Date = 04/03/16 Pct Recovery = 78% Analysis Date = 03/29/16 Pct Recovery = 77% Analysis Date = 03/29/16 Pct Recovery = 77% Analysis Date = 03/24/16 Pct Recovery = 77% Analysis Date = 03/24/16 Pct Recovery = 77% Analysis Date = 03/19/16 Pct Recovery = 77% Analysis Date = 03/19/16 Pct Recovery = 77% Analysis Date = 03/14/16 Pct Recovery = 77% Analysis Date = 03/14/16 Pct Recovery = 77% Analysis Date = 03/09/16 Pct Recovery = 77% Analysis Date = 03/09/16 Pct Recovery = 77% Analysis Date = 03/04/16 Pct Recovery = 77% Analysis Date = 03/04/16 Pct Recovery = 77% Analysis Date = 02/28/16 Pct Recovery = 77% Analysis Date = 02/28/16 Pct Recovery = 77% Analysis Date = 02/23/16 Pct Recovery = 77% Analysis Date = 02/23/16 Pct Recovery = 77% Analysis Date = 02/18/16 Pct Recovery = 77% Analysis Date = 02/18/16 Pct Recovery = 77% Analysis Date = 02/13/16 Pct Recovery = 77% Analysis Date = 02/13/16 Pct Recovery = 77% Analysis Date = 02/08/16 Pct Recovery = 77% Analysis Date = 02/08/16 Pct Recovery = 77% Analysis Date = 02/03/16 Pct Recovery = 77% Analysis Date = 02/03/16 Pct Recovery = 77% Analysis Date = 01/29/16 Pct Recovery = 77% Analysis Date = 01/29/16 Pct Recovery = 77% Analysis Date = 01/24/16 Pct Recovery = 77% Analysis Date = 01/24/16 Pct Recovery = 77% Analysis Date = 01/19/16 Pct Recovery = 77% Analysis Date = 01/19/16 Pct Recovery = 77% Analysis Date = 01/14/16 Pct Recovery = 77% Analysis Date = 01/14/16 Pct Recovery = 77% Analysis Date = 01/09/16 Pct Recovery = 77% Analysis Date = 01/09/16 Pct Recovery = 77% Analysis Date = 01/04/16 Pct Recovery = 77% Analysis Date = 01/04/16 Pct Recovery = 77% Analysis Date = 12/30/15 Pct Recovery = 76% Analysis Date = 12/30/15 Pct Recovery = 76% Analysis Date = 12/25/15 Pct Recovery = 76% Analysis Date = 12/25/15 Pct Recovery = 76% Analysis Date = 12/20/15 Pct Recovery = 76% Analysis Date = 12/20/15 Pct Recovery = 76% Analysis Date = 12/15/15 Pct Recovery = 76% Analysis Date = 12/15/15 Pct Recovery = 76% Analysis Date = 12/10/15 Pct Recovery = 76% Analysis Date = 12/10/15 Pct Recovery = 76% Analysis Date = 12/05/15 Pct Recovery = 76% Analysis Date = 12/05/15 Pct Recovery = 76% Analysis Date = 11/30/15 Pct Recovery = 76% Analysis Date = 11/30/15 Pct Recovery = 76% Analysis Date = 11/25/15 Pct Recovery = 76% Analysis Date = 11/25/15 Pct Recovery = 76% Analysis Date = 11/20/15 Pct Recovery = 76% Analysis Date = 11/20/15 Pct Recovery = 76% Analysis Date = 11/15/15 Pct Recovery = 76% Analysis Date = 11/15/15 Pct Recovery = 76% Analysis Date = 11/10/15 Pct Recovery = 76% Analysis Date = 11/10/15 Pct Recovery = 76% Analysis Date = 11/05/15 Pct Recovery = 76% Analysis Date = 11/05/15 Pct Recovery = 76% Analysis Date = 10/31/15 Pct Recovery = 76% Analysis Date = 10/31/15 Pct Recovery = 76% Analysis Date = 10/26/15 Pct Recovery = 76% Analysis Date = 10/26/15 Pct Recovery = 76% Analysis Date = 10/21/15 Pct Recovery = 76% Analysis Date = 10/21/15 Pct Recovery = 76% Analysis Date = 10/16/15 Pct Recovery = 76% Analysis Date = 10/16/15 Pct Recovery = 76% Analysis Date = 10/11/15 Pct Recovery = 76% Analysis Date = 10/11/15 Pct Recovery = 76% Analysis Date = 10/06/15 Pct Recovery = 76% Analysis Date = 10/06/15 Pct Recovery = 76% Analysis Date = 10/01/15 Pct Recovery = 76% Analysis Date = 10/01/15 Pct Recovery = 76% Analysis Date = 09/26/15 Pct Recovery = 76% Analysis Date = 09/26/15 Pct Recovery = 76% Analysis Date = 09/21/15 Pct Recovery = 76% Analysis Date = 09/21/15 Pct Recovery = 76% Analysis Date = 09/16/15 Pct Recovery = 76% Analysis Date = 09/16/15 Pct Recovery = 76% Analysis Date = 09/11/15 Pct Recovery = 76% Analysis Date = 09/11/15 Pct Recovery = 76% Analysis Date = 09/05/15 Pct Recovery = 76% Analysis Date = 09/05/15 Pct Recovery = 76% Analysis Date = 08/31/15 Pct Recovery = 76% Analysis Date = 08/31/15 Pct Recovery = 76% Analysis Date = 08/26/15 Pct Recovery = 76% Analysis Date = 08/26/15 Pct Recovery = 76% Analysis Date = 08/21/15 Pct Recovery = 76% Analysis Date = 08/21/15 Pct Recovery = 76% Analysis Date = 08/16/15 Pct Recovery = 76% Analysis Date = 08/16/15 Pct Recovery = 76% Analysis Date = 08/11/15 Pct Recovery = 75% Analysis Date = 08/11/15 Pct Recovery = 75% Analysis Date = 08/06/15 Pct Recovery = 75% Analysis Date = 08/06/15 Pct Recovery = 75% Analysis Date = 08/01/15 Pct Recovery = 75% Analysis Date = 08/01/15 Pct Recovery = 75% Analysis Date = 07/27/15 Pct Recovery = 75% Analysis Date = 07/27/15 Pct Recovery = 75% Analysis Date = 07/22/15 Pct Recovery = 75% Analysis Date = 07/22/15 Pct Recovery = 75% Analysis Date = 07/17/15 Pct Recovery = 75% Analysis Date = 07/17/15 Pct Recovery = 75% Analysis Date = 07/12/15 Pct Recovery = 75% Analysis Date = 07/12/15 Pct Recovery = 75% Analysis Date = 07/07/15 Pct Recovery = 75% Analysis Date = 07/07/15 Pct Recovery = 75% Analysis Date = 07/02/15 Pct Recovery = 75% Analysis Date = 07/02/15 Pct Recovery = 75% Analysis Date = 06/27/15 Pct Recovery = 75% Analysis Date = 06/27/15 Pct Recovery = 75% Analysis Date = 06/22/15 Pct Recovery = 75% Analysis Date = 06/22/15 Pct Recovery = 75% Analysis Date = 06/17/15 Pct Recovery = 75% Analysis Date = 06/17/15 Pct Recovery = 75% Analysis Date = 06/12/15 Pct Recovery = 75% Analysis Date = 06/12/15 Pct Recovery = 75% Analysis Date = 06/07/15 Pct Recovery = 75% Analysis Date = 06/07/15 Pct Recovery = 75% Analysis Date = 06/02/15 Pct Recovery = 75% Analysis Date = 06/02/15 Pct Recovery = 75% Analysis Date = 05/28/15 Pct Recovery = 75% Analysis Date = 05/28/15 Pct Recovery = 75% Analysis Date = 05/23/15 Pct Recovery = 75% Analysis Date = 05/23/15 Pct Recovery = 75% Analysis Date = 05/18/15 Pct Recovery = 75% Analysis Date = 05/18/15 Pct Recovery = 75% Analysis Date = 05/13/15 Pct Recovery = 75% Analysis Date = 05/13/15 Pct Recovery = 75% Analysis Date = 05/08/15 Pct Recovery = 75% Analysis Date = 05/08/15 Pct Recovery = 75% Analysis Date = 05/03/15 Pct Recovery = 75% Analysis Date = 05/03/15 Pct Recovery = 75% Analysis Date = 04/28/15 Pct Recovery = 75% Analysis Date = 04/28/15 Pct Recovery = 75% Analysis Date = 04/23/15 Pct Recovery = 75% Analysis Date = 04/23/15 Pct Recovery = 75% Analysis Date = 04/18/15 Pct Recovery = 75% Analysis Date = 04/18/15 Pct Recovery = 75% Analysis Date = 04/13/15 Pct Recovery = 75% Analysis Date = 04/13/15 Pct Recovery = 75% Analysis Date = 04/08/15 Pct Recovery = 74% Analysis Date = 04/08/15 Pct Recovery = 74% Analysis Date = 04/03/15 Pct Recovery = 74% Analysis Date = 04/03/15 Pct Recovery = 74% Analysis Date = 03/29/15 Pct Recovery = 74% Analysis Date = 03/29/15 Pct Recovery = 74% Analysis Date = 03/24/15 Pct Recovery = 74% Analysis Date = 03/24/15 Pct Recovery = 74% Analysis Date = 03/19/15 Pct Recovery = 74% Analysis Date = 03/19/15 Pct Recovery = 74% Analysis Date = 03/14/15 Pct Recovery = 74% Analysis Date = 03/14/15 Pct Recovery = 74% Analysis Date = 03/09/15 Pct Recovery = 74% Analysis Date = 03/09/15 Pct Recovery = 74% Analysis Date = 03/04/15 Pct Recovery = 74% Analysis Date = 03/04/15 Pct Recovery = 74% Analysis Date = 02/27/15 Pct Recovery = 74% Analysis Date = 02/27/15 Pct Recovery = 74% Analysis Date = 02/22/15 Pct Recovery = 74% Analysis Date = 02/22/15 Pct Recovery = 74% Analysis Date = 02/17/15 Pct Recovery = 74% Analysis Date = 02/17/15 Pct Recovery = 74% Analysis Date = 02/12/15 Pct Recovery = 74% Analysis Date = 02/12/15 Pct Recovery = 74% Analysis Date = 02/07/15 Pct Recovery = 74% Analysis Date = 02/07/15 Pct Recovery = 74% Analysis Date = 02/02/15 Pct Recovery = 74% Analysis Date = 02/02/15 Pct Recovery = 74% Analysis Date = 01/28/15 Pct Recovery = 74% Analysis Date = 01/28/15 Pct Recovery = 74% Analysis Date = 01/23/15 Pct Recovery = 74% Analysis Date = 01/23/15 Pct Recovery = 74% Analysis Date = 01/18/15 Pct Recovery = 74% Analysis Date = 01/18/15 Pct Recovery = 74% Analysis Date = 01/13/15 Pct Recovery = 74% Analysis Date = 01/13/15 Pct Recovery = 74% Analysis Date = 01/08/15 Pct Recovery = 74% Analysis Date = 01/08/15 Pct Recovery = 74% Analysis Date = 01/03/15 Pct Recovery = 74% Analysis Date = 01/03/15 Pct Recovery = 74% Analysis Date = 12/29/14 Pct Recovery = 74% Analysis Date = 12/29/14 Pct Recovery = 74% Analysis Date = 12/24/14 Pct Recovery = 74% Analysis Date = 12/24/14 Pct Recovery = 74% Analysis Date = 12/19/14 Pct Recovery = 74% Analysis Date = 12/19/14 Pct Recovery = 74% Analysis Date = 12/14/14 Pct Recovery = 74% Analysis Date = 12/14/14 Pct Recovery = 74% Analysis Date = 12/09/14 Pct Recovery = 74% Analysis Date = 12/09/14 Pct Recovery = 74% Analysis Date = 12/04/14 Pct Recovery = 74% Analysis Date = 12/04/14 Pct Recovery = 74% Analysis Date = 11/29/14 Pct Recovery = 74% Analysis Date = 11/29/14 Pct Recovery = 74% Analysis Date = 11/24/14 Pct Recovery = 74% Analysis Date = 11/24/14 Pct Recovery = 74% Analysis Date = 11/19/14 Pct Recovery = 74% Analysis Date = 11/19/14 Pct Recovery = 74% Analysis Date = 11/14/14 Pct Recovery = 74% Analysis Date = 11/14/14 Pct Recovery = 74% Analysis Date = 11/09/14 Pct Recovery = 74% Analysis Date = 11/09/14 Pct Recovery = 74% Analysis Date = 11/04/14 Pct Recovery = 73% Analysis Date = 11/04/14 Pct Recovery = 73% Analysis Date = 10/30/14 Pct Recovery = 73% Analysis Date = 10/30/14 Pct Recovery = 73% Analysis Date = 10/25/14 Pct Recovery = 73% Analysis Date = 10/25/14 Pct Recovery = 73% Analysis Date = 10/20/14 Pct Recovery = 73% Analysis Date = 10/20/14 Pct Recovery = 73% Analysis Date = 10/15/14 Pct Recovery = 73% Analysis Date = 10/15/14 Pct Recovery = 73% Analysis Date = 10/10/14 Pct Recovery = 73% Analysis Date = 10/10/14 Pct Recovery = 73% Analysis Date = 10/05/14 Pct Recovery = 73% Analysis Date = 10/05/14 Pct Recovery = 73% Analysis Date = 09/30/14 Pct Recovery = 73% Analysis Date = 09/30/14 Pct Recovery = 73% Analysis Date = 09/25/14 Pct Recovery = 73% Analysis Date = 09/25/14 Pct Recovery = 73% Analysis Date = 09/20/14 Pct Recovery = 73% Analysis Date = 09/20/14 Pct Recovery = 73% Analysis Date = 09/15/14 Pct Recovery = 73% Analysis Date = 09/15/14 Pct Recovery = 73% Analysis Date = 09/10/14 Pct Recovery = 73% Analysis Date = 09/10/14 Pct Recovery = 73% Analysis Date = 09/05/14 Pct Recovery = 73% Analysis Date = 09/05/14 Pct Recovery = 73% Analysis Date = 08/31/14 Pct Recovery = 73% Analysis Date = 08/31/14 Pct Recovery = 73% Analysis Date = 08/26/14 Pct Recovery = 73% Analysis Date = 08/26/14 Pct Recovery = 73% Analysis Date = 08/21/14 Pct Recovery = 73% Analysis Date = 08/21/14 Pct Recovery = 73% Analysis Date = 08/16/14 Pct Recovery = 73% Analysis Date = 08/16/14 Pct Recovery = 73% Analysis Date = 08/11/14 Pct Recovery = 73% Analysis Date = 08/11/14 Pct Recovery = 73% Analysis Date = 08/06/14 Pct Recovery = 73% Analysis Date = 08/06/14 Pct Recovery = 73% Analysis Date = 08/01/14 Pct Recovery = 73% Analysis Date = 08/01/14 Pct Recovery = 73% Analysis Date = 07/27/14 Pct Recovery = 73% Analysis Date = 07/27/14 Pct Recovery = 73% Analysis Date = 07/22/14 Pct Recovery = 73% Analysis Date = 07/22/14 Pct Recovery = 73% Analysis Date = 07/17/14 Pct Recovery = 73% Analysis Date = 07/17/14 Pct Recovery = 73% Analysis Date = 07/12/14 Pct Recovery = 73% Analysis Date = 07/12/14 Pct Recovery = 73% Analysis Date = 07/07/14 Pct Recovery = 73% Analysis Date = 07/07/14 Pct Recovery = 73% Analysis Date = 07/02/14 Pct Recovery = 73% Analysis Date = 07/02/14 Pct Recovery = 73% Analysis Date = 06/27/14 Pct Recovery = 73% Analysis Date = 06/27/14 Pct Recovery = 73% Analysis Date = 06/22/14 Pct Recovery = 73% Analysis Date = 06/22/14 Pct Recovery = 73% Analysis Date = 06/17/14 Pct Recovery = 73% Analysis Date = 06/17/14 Pct Recovery = 73% Analysis Date = 06/12/14 Pct Recovery = 73% Analysis Date = 06/12/14 Pct Recovery = 73% Analysis Date = 06/07/14 Pct Recovery = 73% Analysis Date = 06/07/14 Pct Recovery = 73% Analysis Date = 06/02/14 Pct Recovery = 73% Analysis Date = 06/02/14 Pct Recovery = 73% Analysis Date = 05/28/14 Pct Recovery = 73% Analysis Date = 05/28/14 Pct Recovery = 73% Analysis Date = 05/23/14 Pct Recovery = 73% Analysis Date = 05/23/14 Pct Recovery = 73% Analysis Date = 05/18/14 Pct Recovery = 72% Analysis Date = 05/18/14 Pct Recovery = 72% Analysis Date = 05/13/14 Pct Recovery = 72% Analysis Date = 05/13/14 Pct Recovery = 72% Analysis Date = 05/08/14 Pct Recovery = 72% Analysis Date = 05/08/14 Pct Recovery = 72% Analysis Date = 05/03/14 Pct Recovery = 72% Analysis Date = 05/03/14 Pct Recovery = 72% Analysis Date = 04/28/14 Pct Recovery = 72% Analysis Date = 04/28/14 Pct Recovery = 72% Analysis Date = 04/23/14 Pct Recovery = 72% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
CARBAMAZEPINE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 15 71% 12% 71% 13%
>= Reporting Level 61 78% 11% 78% 8%
Total 76 77% 11% 77% 9%

Sample Statistics
CARBAMAZEPINE

Characteristic N % % Basis
Plotted 76 99% Spiked
Estimated Values 5 6% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 1 1% Spiked
Spiked 77 .  
False Negatives 0 0% 0 out of 77
Not Spiked 38 .  
False Positives 1 3% 1 out of 38

BQS OBSP Determination:
CARISOPRODOL
METHOD: 2440 , TESTIDCODE: 67498LCM56
Open Data Set

Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 78% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 82% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 80 µl & ERA 0406-15-08: 80 µl Pct Recovery = 73% Analysis Date = 11/04/15 SpikeMix = Abs 052215: 80 µl & Abs 050115: 80 µl Pct Recovery = 82% Analysis Date = 09/24/16 SpikeMix = Crescent EN160610015: 80 µl & Abs 061416: 80 µl Pct Recovery = 85% Analysis Date = 09/24/16 SpikeMix = Abs 061416: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 78% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 96% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 90% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 99% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 92% Analysis Date = 11/18/16 SpikeMix = ERA 04281604: 80 µl & ERA 04281603: 80 µl Pct Recovery = 74% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & ERA 04281604: 80 µl Pct Recovery = 74% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-04: 15 µl & Abs 041814: 15 µl Pct Recovery = 61% Analysis Date = 12/06/14 SpikeMix = ERA 0318-14-02: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 80% Analysis Date = 10/25/14 SpikeMix = Abs 041614: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 71% Analysis Date = 10/11/14 SpikeMix = ERA 0318-14-02: 60 µl & ERA 0319-14-04: 60 µl Pct Recovery = 57% Analysis Date = 08/28/14 SpikeMix = ERA 0319-14-04: 60 µl & ERA 0319-14-05: 60 µl Pct Recovery = 54% Analysis Date = 05/07/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 100% Analysis Date = 03/11/15 SpikeMix = ERA 0318-14-02: 15 µl & Abs 041714: 15 µl Pct Recovery = 94% Analysis Date = 01/16/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 87% Analysis Date = 12/06/14 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 64% Analysis Date = 08/21/14 SpikeMix = ERA 0318-14-02: 60 µl & Abs 041714: 60 µl Pct Recovery = 72% Analysis Date = 07/12/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 83% Analysis Date = 06/11/14 SpikeMix = Abs 041614: 60 µl & Abs 041714: 60 µl Pct Recovery = 78% Analysis Date = 05/21/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 86% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 83% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 73% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 86% Analysis Date = 02/23/16 SpikeMix = Abs 052215: 40 µl & Abs 050115: 40 µl Pct Recovery = 74% Analysis Date = 07/30/15 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 71% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 72% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 72% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 71% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 81% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 84% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 78% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 69% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 64% Analysis Date = 04/30/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 77% Analysis Date = 04/10/15 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 83% Analysis Date = 02/10/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 79% Analysis Date = 12/07/14 SpikeMix = ERA 0318-14-02: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 51% Analysis Date = 10/11/14 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 65% Analysis Date = 11/04/14 SpikeMix = Abs 041714: 8 µl & ERA 0319-14-05: 8 µl Pct Recovery = 54% Analysis Date = 09/12/14 SpikeMix = Abs 041614: 30 µl & ERA 0319-14-04: 30 µl Pct Recovery = 54% Analysis Date = 08/16/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 70% Analysis Date = 07/13/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 88% Analysis Date = 04/23/14 SpikeMix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.2: 20 µl Pct Recovery = 84% Analysis Date = 10/10/14 SpikeMix = Abs 041714: 30 µl & Abs 041814: 30 µl Pct Recovery = 63% Analysis Date = 07/20/14 SpikeMix = ERA 0318-14-02: 30 µl & Abs 041714: 30 µl Pct Recovery = 74% Analysis Date = 06/28/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 77% Analysis Date = 05/17/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 72% Analysis Date = 11/25/15 SpikeMix = Abs 050115: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 89% Analysis Date = 11/24/15 SpikeMix = ERA 0406-15-09: 20 µl & Abs 050115: 20 µl Pct Recovery = 88% Analysis Date = 08/11/15 SpikeMix = Abs 050115: 20 µl & Abs 051315: 20 µl Pct Recovery = 64% Analysis Date = 07/09/15 SpikeMix = Abs 050115: 20 µl & Abs 052215: 20 µl Pct Recovery = 81% Analysis Date = 06/09/15 SpikeMix = Abs 051315: 20 µl & Abs 050115: 20 µl Pct Recovery = 71% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 69% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 68% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 84% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 101% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 81% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 84% Analysis Date = 01/04/17 Pct Recovery = 79% Analysis Date = 12/31/16 Pct Recovery = 79% Analysis Date = 12/31/16 Pct Recovery = 79% Analysis Date = 12/26/16 Pct Recovery = 79% Analysis Date = 12/26/16 Pct Recovery = 79% Analysis Date = 12/21/16 Pct Recovery = 79% Analysis Date = 12/21/16 Pct Recovery = 79% Analysis Date = 12/16/16 Pct Recovery = 79% Analysis Date = 12/16/16 Pct Recovery = 79% Analysis Date = 12/11/16 Pct Recovery = 79% Analysis Date = 12/11/16 Pct Recovery = 79% Analysis Date = 12/06/16 Pct Recovery = 79% Analysis Date = 12/06/16 Pct Recovery = 79% Analysis Date = 12/01/16 Pct Recovery = 79% Analysis Date = 12/01/16 Pct Recovery = 79% Analysis Date = 11/26/16 Pct Recovery = 79% Analysis Date = 11/26/16 Pct Recovery = 79% Analysis Date = 11/21/16 Pct Recovery = 79% Analysis Date = 11/21/16 Pct Recovery = 79% Analysis Date = 11/16/16 Pct Recovery = 79% Analysis Date = 11/16/16 Pct Recovery = 79% Analysis Date = 11/11/16 Pct Recovery = 79% Analysis Date = 11/11/16 Pct Recovery = 79% Analysis Date = 11/06/16 Pct Recovery = 79% Analysis Date = 11/06/16 Pct Recovery = 79% Analysis Date = 11/01/16 Pct Recovery = 79% Analysis Date = 11/01/16 Pct Recovery = 79% Analysis Date = 10/27/16 Pct Recovery = 80% Analysis Date = 10/27/16 Pct Recovery = 80% Analysis Date = 10/22/16 Pct Recovery = 80% Analysis Date = 10/22/16 Pct Recovery = 80% Analysis Date = 10/17/16 Pct Recovery = 80% Analysis Date = 10/17/16 Pct Recovery = 80% Analysis Date = 10/13/16 Pct Recovery = 80% Analysis Date = 10/13/16 Pct Recovery = 80% Analysis Date = 10/08/16 Pct Recovery = 80% Analysis Date = 10/08/16 Pct Recovery = 80% Analysis Date = 10/03/16 Pct Recovery = 80% Analysis Date = 10/03/16 Pct Recovery = 80% Analysis Date = 09/28/16 Pct Recovery = 80% Analysis Date = 09/28/16 Pct Recovery = 80% Analysis Date = 09/23/16 Pct Recovery = 80% Analysis Date = 09/23/16 Pct Recovery = 80% Analysis Date = 09/18/16 Pct Recovery = 80% Analysis Date = 09/18/16 Pct Recovery = 80% Analysis Date = 09/13/16 Pct Recovery = 80% Analysis Date = 09/13/16 Pct Recovery = 80% Analysis Date = 09/08/16 Pct Recovery = 80% Analysis Date = 09/08/16 Pct Recovery = 80% Analysis Date = 09/03/16 Pct Recovery = 80% Analysis Date = 09/03/16 Pct Recovery = 80% Analysis Date = 08/29/16 Pct Recovery = 80% Analysis Date = 08/29/16 Pct Recovery = 80% Analysis Date = 08/24/16 Pct Recovery = 80% Analysis Date = 08/24/16 Pct Recovery = 80% Analysis Date = 08/19/16 Pct Recovery = 80% Analysis Date = 08/19/16 Pct Recovery = 80% Analysis Date = 08/14/16 Pct Recovery = 80% Analysis Date = 08/14/16 Pct Recovery = 80% Analysis Date = 08/09/16 Pct Recovery = 80% Analysis Date = 08/09/16 Pct Recovery = 80% Analysis Date = 08/04/16 Pct Recovery = 80% Analysis Date = 08/04/16 Pct Recovery = 80% Analysis Date = 07/30/16 Pct Recovery = 80% Analysis Date = 07/30/16 Pct Recovery = 80% Analysis Date = 07/25/16 Pct Recovery = 80% Analysis Date = 07/25/16 Pct Recovery = 80% Analysis Date = 07/21/16 Pct Recovery = 80% Analysis Date = 07/21/16 Pct Recovery = 80% Analysis Date = 07/16/16 Pct Recovery = 80% Analysis Date = 07/16/16 Pct Recovery = 80% Analysis Date = 07/11/16 Pct Recovery = 80% Analysis Date = 07/11/16 Pct Recovery = 80% Analysis Date = 07/06/16 Pct Recovery = 80% Analysis Date = 07/06/16 Pct Recovery = 80% Analysis Date = 07/01/16 Pct Recovery = 80% Analysis Date = 07/01/16 Pct Recovery = 80% Analysis Date = 06/26/16 Pct Recovery = 80% Analysis Date = 06/26/16 Pct Recovery = 80% Analysis Date = 06/21/16 Pct Recovery = 80% Analysis Date = 06/21/16 Pct Recovery = 80% Analysis Date = 06/16/16 Pct Recovery = 80% Analysis Date = 06/16/16 Pct Recovery = 80% Analysis Date = 06/11/16 Pct Recovery = 80% Analysis Date = 06/11/16 Pct Recovery = 80% Analysis Date = 06/06/16 Pct Recovery = 80% Analysis Date = 06/06/16 Pct Recovery = 80% Analysis Date = 06/01/16 Pct Recovery = 80% Analysis Date = 06/01/16 Pct Recovery = 80% Analysis Date = 05/27/16 Pct Recovery = 80% Analysis Date = 05/27/16 Pct Recovery = 80% Analysis Date = 05/22/16 Pct Recovery = 80% Analysis Date = 05/22/16 Pct Recovery = 80% Analysis Date = 05/17/16 Pct Recovery = 80% Analysis Date = 05/17/16 Pct Recovery = 80% Analysis Date = 05/12/16 Pct Recovery = 80% Analysis Date = 05/12/16 Pct Recovery = 80% Analysis Date = 05/07/16 Pct Recovery = 80% Analysis Date = 05/07/16 Pct Recovery = 80% Analysis Date = 05/02/16 Pct Recovery = 81% Analysis Date = 05/02/16 Pct Recovery = 81% Analysis Date = 04/28/16 Pct Recovery = 81% Analysis Date = 04/28/16 Pct Recovery = 81% Analysis Date = 04/23/16 Pct Recovery = 81% Analysis Date = 04/23/16 Pct Recovery = 81% Analysis Date = 04/18/16 Pct Recovery = 81% Analysis Date = 04/18/16 Pct Recovery = 81% Analysis Date = 04/13/16 Pct Recovery = 81% Analysis Date = 04/13/16 Pct Recovery = 81% Analysis Date = 04/08/16 Pct Recovery = 81% Analysis Date = 04/08/16 Pct Recovery = 81% Analysis Date = 04/03/16 Pct Recovery = 81% Analysis Date = 04/03/16 Pct Recovery = 81% Analysis Date = 03/29/16 Pct Recovery = 81% Analysis Date = 03/29/16 Pct Recovery = 81% Analysis Date = 03/24/16 Pct Recovery = 81% Analysis Date = 03/24/16 Pct Recovery = 81% Analysis Date = 03/19/16 Pct Recovery = 81% Analysis Date = 03/19/16 Pct Recovery = 81% Analysis Date = 03/14/16 Pct Recovery = 81% Analysis Date = 03/14/16 Pct Recovery = 81% Analysis Date = 03/09/16 Pct Recovery = 81% Analysis Date = 03/09/16 Pct Recovery = 81% Analysis Date = 03/04/16 Pct Recovery = 81% Analysis Date = 03/04/16 Pct Recovery = 81% Analysis Date = 02/28/16 Pct Recovery = 81% Analysis Date = 02/28/16 Pct Recovery = 81% Analysis Date = 02/23/16 Pct Recovery = 81% Analysis Date = 02/23/16 Pct Recovery = 81% Analysis Date = 02/18/16 Pct Recovery = 81% Analysis Date = 02/18/16 Pct Recovery = 81% Analysis Date = 02/13/16 Pct Recovery = 81% Analysis Date = 02/13/16 Pct Recovery = 81% Analysis Date = 02/09/16 Pct Recovery = 81% Analysis Date = 02/09/16 Pct Recovery = 81% Analysis Date = 02/04/16 Pct Recovery = 81% Analysis Date = 02/04/16 Pct Recovery = 81% Analysis Date = 01/30/16 Pct Recovery = 81% Analysis Date = 01/30/16 Pct Recovery = 81% Analysis Date = 01/25/16 Pct Recovery = 81% Analysis Date = 01/25/16 Pct Recovery = 81% Analysis Date = 01/20/16 Pct Recovery = 81% Analysis Date = 01/20/16 Pct Recovery = 81% Analysis Date = 01/15/16 Pct Recovery = 81% Analysis Date = 01/15/16 Pct Recovery = 81% Analysis Date = 01/10/16 Pct Recovery = 80% Analysis Date = 01/10/16 Pct Recovery = 80% Analysis Date = 01/05/16 Pct Recovery = 80% Analysis Date = 01/05/16 Pct Recovery = 80% Analysis Date = 12/31/15 Pct Recovery = 80% Analysis Date = 12/31/15 Pct Recovery = 80% Analysis Date = 12/26/15 Pct Recovery = 80% Analysis Date = 12/26/15 Pct Recovery = 80% Analysis Date = 12/21/15 Pct Recovery = 80% Analysis Date = 12/21/15 Pct Recovery = 80% Analysis Date = 12/16/15 Pct Recovery = 80% Analysis Date = 12/16/15 Pct Recovery = 80% Analysis Date = 12/11/15 Pct Recovery = 80% Analysis Date = 12/11/15 Pct Recovery = 80% Analysis Date = 12/06/15 Pct Recovery = 80% Analysis Date = 12/06/15 Pct Recovery = 80% Analysis Date = 12/01/15 Pct Recovery = 80% Analysis Date = 12/01/15 Pct Recovery = 80% Analysis Date = 11/26/15 Pct Recovery = 80% Analysis Date = 11/26/15 Pct Recovery = 80% Analysis Date = 11/21/15 Pct Recovery = 80% Analysis Date = 11/21/15 Pct Recovery = 80% Analysis Date = 11/17/15 Pct Recovery = 80% Analysis Date = 11/17/15 Pct Recovery = 80% Analysis Date = 11/12/15 Pct Recovery = 80% Analysis Date = 11/12/15 Pct Recovery = 80% Analysis Date = 11/07/15 Pct Recovery = 80% Analysis Date = 11/07/15 Pct Recovery = 80% Analysis Date = 11/02/15 Pct Recovery = 80% Analysis Date = 11/02/15 Pct Recovery = 80% Analysis Date = 10/28/15 Pct Recovery = 80% Analysis Date = 10/28/15 Pct Recovery = 80% Analysis Date = 10/23/15 Pct Recovery = 80% Analysis Date = 10/23/15 Pct Recovery = 80% Analysis Date = 10/18/15 Pct Recovery = 80% Analysis Date = 10/18/15 Pct Recovery = 80% Analysis Date = 10/13/15 Pct Recovery = 80% Analysis Date = 10/13/15 Pct Recovery = 80% Analysis Date = 10/08/15 Pct Recovery = 80% Analysis Date = 10/08/15 Pct Recovery = 80% Analysis Date = 10/03/15 Pct Recovery = 79% Analysis Date = 10/03/15 Pct Recovery = 79% Analysis Date = 09/28/15 Pct Recovery = 79% Analysis Date = 09/28/15 Pct Recovery = 79% Analysis Date = 09/23/15 Pct Recovery = 79% Analysis Date = 09/23/15 Pct Recovery = 79% Analysis Date = 09/18/15 Pct Recovery = 79% Analysis Date = 09/18/15 Pct Recovery = 79% Analysis Date = 09/13/15 Pct Recovery = 79% Analysis Date = 09/13/15 Pct Recovery = 79% Analysis Date = 09/08/15 Pct Recovery = 79% Analysis Date = 09/08/15 Pct Recovery = 79% Analysis Date = 09/03/15 Pct Recovery = 79% Analysis Date = 09/03/15 Pct Recovery = 79% Analysis Date = 08/29/15 Pct Recovery = 79% Analysis Date = 08/29/15 Pct Recovery = 79% Analysis Date = 08/25/15 Pct Recovery = 79% Analysis Date = 08/25/15 Pct Recovery = 79% Analysis Date = 08/20/15 Pct Recovery = 79% Analysis Date = 08/20/15 Pct Recovery = 79% Analysis Date = 08/15/15 Pct Recovery = 78% Analysis Date = 08/15/15 Pct Recovery = 78% Analysis Date = 08/10/15 Pct Recovery = 78% Analysis Date = 08/10/15 Pct Recovery = 78% Analysis Date = 08/05/15 Pct Recovery = 78% Analysis Date = 08/05/15 Pct Recovery = 78% Analysis Date = 07/31/15 Pct Recovery = 78% Analysis Date = 07/31/15 Pct Recovery = 78% Analysis Date = 07/26/15 Pct Recovery = 78% Analysis Date = 07/26/15 Pct Recovery = 78% Analysis Date = 07/21/15 Pct Recovery = 78% Analysis Date = 07/21/15 Pct Recovery = 78% Analysis Date = 07/16/15 Pct Recovery = 78% Analysis Date = 07/16/15 Pct Recovery = 78% Analysis Date = 07/11/15 Pct Recovery = 78% Analysis Date = 07/11/15 Pct Recovery = 78% Analysis Date = 07/06/15 Pct Recovery = 78% Analysis Date = 07/06/15 Pct Recovery = 78% Analysis Date = 07/01/15 Pct Recovery = 78% Analysis Date = 07/01/15 Pct Recovery = 78% Analysis Date = 06/26/15 Pct Recovery = 77% Analysis Date = 06/26/15 Pct Recovery = 77% Analysis Date = 06/21/15 Pct Recovery = 77% Analysis Date = 06/21/15 Pct Recovery = 77% Analysis Date = 06/16/15 Pct Recovery = 77% Analysis Date = 06/16/15 Pct Recovery = 77% Analysis Date = 06/11/15 Pct Recovery = 77% Analysis Date = 06/11/15 Pct Recovery = 77% Analysis Date = 06/07/15 Pct Recovery = 77% Analysis Date = 06/07/15 Pct Recovery = 77% Analysis Date = 06/02/15 Pct Recovery = 77% Analysis Date = 06/02/15 Pct Recovery = 77% Analysis Date = 05/28/15 Pct Recovery = 77% Analysis Date = 05/28/15 Pct Recovery = 77% Analysis Date = 05/23/15 Pct Recovery = 77% Analysis Date = 05/23/15 Pct Recovery = 77% Analysis Date = 05/18/15 Pct Recovery = 76% Analysis Date = 05/18/15 Pct Recovery = 76% Analysis Date = 05/13/15 Pct Recovery = 76% Analysis Date = 05/13/15 Pct Recovery = 76% Analysis Date = 05/08/15 Pct Recovery = 76% Analysis Date = 05/08/15 Pct Recovery = 76% Analysis Date = 05/03/15 Pct Recovery = 76% Analysis Date = 05/03/15 Pct Recovery = 76% Analysis Date = 04/28/15 Pct Recovery = 76% Analysis Date = 04/28/15 Pct Recovery = 76% Analysis Date = 04/23/15 Pct Recovery = 76% Analysis Date = 04/23/15 Pct Recovery = 76% Analysis Date = 04/18/15 Pct Recovery = 76% Analysis Date = 04/18/15 Pct Recovery = 76% Analysis Date = 04/13/15 Pct Recovery = 75% Analysis Date = 04/13/15 Pct Recovery = 75% Analysis Date = 04/08/15 Pct Recovery = 75% Analysis Date = 04/08/15 Pct Recovery = 75% Analysis Date = 04/03/15 Pct Recovery = 75% Analysis Date = 04/03/15 Pct Recovery = 75% Analysis Date = 03/29/15 Pct Recovery = 75% Analysis Date = 03/29/15 Pct Recovery = 75% Analysis Date = 03/24/15 Pct Recovery = 75% Analysis Date = 03/24/15 Pct Recovery = 75% Analysis Date = 03/19/15 Pct Recovery = 75% Analysis Date = 03/19/15 Pct Recovery = 75% Analysis Date = 03/15/15 Pct Recovery = 74% Analysis Date = 03/15/15 Pct Recovery = 74% Analysis Date = 03/10/15 Pct Recovery = 74% Analysis Date = 03/10/15 Pct Recovery = 74% Analysis Date = 03/05/15 Pct Recovery = 74% Analysis Date = 03/05/15 Pct Recovery = 74% Analysis Date = 02/28/15 Pct Recovery = 74% Analysis Date = 02/28/15 Pct Recovery = 74% Analysis Date = 02/23/15 Pct Recovery = 74% Analysis Date = 02/23/15 Pct Recovery = 74% Analysis Date = 02/18/15 Pct Recovery = 74% Analysis Date = 02/18/15 Pct Recovery = 74% Analysis Date = 02/13/15 Pct Recovery = 74% Analysis Date = 02/13/15 Pct Recovery = 74% Analysis Date = 02/08/15 Pct Recovery = 74% Analysis Date = 02/08/15 Pct Recovery = 74% Analysis Date = 02/03/15 Pct Recovery = 74% Analysis Date = 02/03/15 Pct Recovery = 74% Analysis Date = 01/29/15 Pct Recovery = 74% Analysis Date = 01/29/15 Pct Recovery = 74% Analysis Date = 01/24/15 Pct Recovery = 74% Analysis Date = 01/24/15 Pct Recovery = 74% Analysis Date = 01/19/15 Pct Recovery = 74% Analysis Date = 01/19/15 Pct Recovery = 74% Analysis Date = 01/14/15 Pct Recovery = 74% Analysis Date = 01/14/15 Pct Recovery = 74% Analysis Date = 01/09/15 Pct Recovery = 74% Analysis Date = 01/09/15 Pct Recovery = 74% Analysis Date = 01/04/15 Pct Recovery = 73% Analysis Date = 01/04/15 Pct Recovery = 73% Analysis Date = 12/30/14 Pct Recovery = 73% Analysis Date = 12/30/14 Pct Recovery = 73% Analysis Date = 12/25/14 Pct Recovery = 73% Analysis Date = 12/25/14 Pct Recovery = 73% Analysis Date = 12/21/14 Pct Recovery = 73% Analysis Date = 12/21/14 Pct Recovery = 73% Analysis Date = 12/16/14 Pct Recovery = 73% Analysis Date = 12/16/14 Pct Recovery = 73% Analysis Date = 12/11/14 Pct Recovery = 73% Analysis Date = 12/11/14 Pct Recovery = 73% Analysis Date = 12/06/14 Pct Recovery = 73% Analysis Date = 12/06/14 Pct Recovery = 73% Analysis Date = 12/01/14 Pct Recovery = 73% Analysis Date = 12/01/14 Pct Recovery = 73% Analysis Date = 11/26/14 Pct Recovery = 73% Analysis Date = 11/26/14 Pct Recovery = 73% Analysis Date = 11/21/14 Pct Recovery = 73% Analysis Date = 11/21/14 Pct Recovery = 73% Analysis Date = 11/16/14 Pct Recovery = 73% Analysis Date = 11/16/14 Pct Recovery = 73% Analysis Date = 11/11/14 Pct Recovery = 73% Analysis Date = 11/11/14 Pct Recovery = 73% Analysis Date = 11/06/14 Pct Recovery = 73% Analysis Date = 11/06/14 Pct Recovery = 73% Analysis Date = 11/01/14 Pct Recovery = 73% Analysis Date = 11/01/14 Pct Recovery = 73% Analysis Date = 10/27/14 Pct Recovery = 73% Analysis Date = 10/27/14 Pct Recovery = 73% Analysis Date = 10/22/14 Pct Recovery = 73% Analysis Date = 10/22/14 Pct Recovery = 73% Analysis Date = 10/17/14 Pct Recovery = 73% Analysis Date = 10/17/14 Pct Recovery = 73% Analysis Date = 10/12/14 Pct Recovery = 73% Analysis Date = 10/12/14 Pct Recovery = 73% Analysis Date = 10/07/14 Pct Recovery = 73% Analysis Date = 10/07/14 Pct Recovery = 73% Analysis Date = 10/03/14 Pct Recovery = 73% Analysis Date = 10/03/14 Pct Recovery = 73% Analysis Date = 09/28/14 Pct Recovery = 73% Analysis Date = 09/28/14 Pct Recovery = 73% Analysis Date = 09/23/14 Pct Recovery = 73% Analysis Date = 09/23/14 Pct Recovery = 73% Analysis Date = 09/18/14 Pct Recovery = 73% Analysis Date = 09/18/14 Pct Recovery = 73% Analysis Date = 09/13/14 Pct Recovery = 73% Analysis Date = 09/13/14 Pct Recovery = 73% Analysis Date = 09/08/14 Pct Recovery = 72% Analysis Date = 09/08/14 Pct Recovery = 72% Analysis Date = 09/03/14 Pct Recovery = 72% Analysis Date = 09/03/14 Pct Recovery = 72% Analysis Date = 08/29/14 Pct Recovery = 72% Analysis Date = 08/29/14 Pct Recovery = 72% Analysis Date = 08/24/14 Pct Recovery = 72% Analysis Date = 08/24/14 Pct Recovery = 72% Analysis Date = 08/19/14 Pct Recovery = 72% Analysis Date = 08/19/14 Pct Recovery = 72% Analysis Date = 08/14/14 Pct Recovery = 72% Analysis Date = 08/14/14 Pct Recovery = 72% Analysis Date = 08/09/14 Pct Recovery = 72% Analysis Date = 08/09/14 Pct Recovery = 72% Analysis Date = 08/04/14 Pct Recovery = 72% Analysis Date = 08/04/14 Pct Recovery = 72% Analysis Date = 07/30/14 Pct Recovery = 72% Analysis Date = 07/30/14 Pct Recovery = 72% Analysis Date = 07/25/14 Pct Recovery = 72% Analysis Date = 07/25/14 Pct Recovery = 72% Analysis Date = 07/20/14 Pct Recovery = 72% Analysis Date = 07/20/14 Pct Recovery = 72% Analysis Date = 07/15/14 Pct Recovery = 72% Analysis Date = 07/15/14 Pct Recovery = 72% Analysis Date = 07/11/14 Pct Recovery = 72% Analysis Date = 07/11/14 Pct Recovery = 72% Analysis Date = 07/06/14 Pct Recovery = 72% Analysis Date = 07/06/14 Pct Recovery = 72% Analysis Date = 07/01/14 Pct Recovery = 72% Analysis Date = 07/01/14 Pct Recovery = 72% Analysis Date = 06/26/14 Pct Recovery = 72% Analysis Date = 06/26/14 Pct Recovery = 72% Analysis Date = 06/21/14 Pct Recovery = 72% Analysis Date = 06/21/14 Pct Recovery = 72% Analysis Date = 06/16/14 Pct Recovery = 72% Analysis Date = 06/16/14 Pct Recovery = 72% Analysis Date = 06/11/14 Pct Recovery = 72% Analysis Date = 06/11/14 Pct Recovery = 72% Analysis Date = 06/06/14 Pct Recovery = 72% Analysis Date = 06/06/14 Pct Recovery = 72% Analysis Date = 06/01/14 Pct Recovery = 72% Analysis Date = 06/01/14 Pct Recovery = 72% Analysis Date = 05/27/14 Pct Recovery = 72% Analysis Date = 05/27/14 Pct Recovery = 72% Analysis Date = 05/22/14 Pct Recovery = 72% Analysis Date = 05/22/14 Pct Recovery = 72% Analysis Date = 05/17/14 Pct Recovery = 72% Analysis Date = 05/17/14 Pct Recovery = 72% Analysis Date = 05/12/14 Pct Recovery = 72% Analysis Date = 05/12/14 Pct Recovery = 72% Analysis Date = 05/07/14 Pct Recovery = 72% Analysis Date = 05/07/14 Pct Recovery = 72% Analysis Date = 05/02/14 Pct Recovery = 72% Analysis Date = 05/02/14 Pct Recovery = 72% Analysis Date = 04/27/14 Pct Recovery = 72% Analysis Date = 04/27/14 Pct Recovery = 72% Analysis Date = 04/23/14 Pct Recovery = 72% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
CARISOPRODOL

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 6 81% 12% 83% 11%
>= Reporting Level 57 76% 11% 77% 10%
Total 63 77% 11% 78% 10%

Sample Statistics
CARISOPRODOL

Characteristic N % % Basis
Plotted 63 97% Spiked
Estimated Values 7 11% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 65 .  
False Negatives 2 3% 2 out of 65
Not Spiked 50 .  
False Positives 1 2% 1 out of 50

BQS OBSP Determination:
CHLORPHENIRAMINE
METHOD: 2440 , TESTIDCODE: 67497LCM56
Open Data Set

Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 50% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 52% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 26% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 46% Analysis Date = 12/06/14 SpikeMix = ERA 0318-14-02: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 42% Analysis Date = 10/25/14 SpikeMix = Abs 041614: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 52% Analysis Date = 10/11/14 SpikeMix = ERA 0318-14-02: 60 µl & ERA 0319-14-04: 60 µl Pct Recovery = 56% Analysis Date = 08/28/14 SpikeMix = ERA 0319-14-04: 60 µl & ERA 0319-14-05: 60 µl Pct Recovery = 43% Analysis Date = 05/07/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 40% Analysis Date = 03/11/15 SpikeMix = ERA 0318-14-02: 15 µl & Abs 041714: 15 µl Pct Recovery = 66% Analysis Date = 01/16/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 47% Analysis Date = 12/06/14 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 48% Analysis Date = 08/21/14 SpikeMix = ERA 0318-14-02: 60 µl & Abs 041714: 60 µl Pct Recovery = 24% Analysis Date = 07/12/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 35% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 32% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 39% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 40% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 53% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 42% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 41% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 40% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 33% Analysis Date = 04/30/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 37% Analysis Date = 04/10/15 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 33% Analysis Date = 12/07/14 SpikeMix = ERA 0318-14-02: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 69% Analysis Date = 10/11/14 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 27% Analysis Date = 09/12/14 SpikeMix = Abs 041614: 30 µl & ERA 0319-14-04: 30 µl Pct Recovery = 33% Analysis Date = 08/16/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 41% Analysis Date = 07/13/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 20% Analysis Date = 10/10/14 SpikeMix = Abs 041714: 30 µl & Abs 041814: 30 µl Pct Recovery = 59% Analysis Date = 07/20/14 SpikeMix = ERA 0318-14-02: 30 µl & Abs 041714: 30 µl Pct Recovery = 28% Analysis Date = 06/28/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 39% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 38% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 33% Analysis Date = 11/18/16 SpikeMix = ERA 04281604: 80 µl & ERA 04281603: 80 µl Pct Recovery = 46% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & ERA 04281604: 80 µl Pct Recovery = 41% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 48% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 39% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 31% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 27% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 67% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 78% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 53% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 46% Analysis Date = 01/19/17 Pct Recovery = 50% Analysis Date = 01/14/17 Pct Recovery = 50% Analysis Date = 01/14/17 Pct Recovery = 50% Analysis Date = 01/09/17 Pct Recovery = 50% Analysis Date = 01/09/17 Pct Recovery = 50% Analysis Date = 01/04/17 Pct Recovery = 49% Analysis Date = 01/04/17 Pct Recovery = 49% Analysis Date = 12/31/16 Pct Recovery = 49% Analysis Date = 12/31/16 Pct Recovery = 49% Analysis Date = 12/26/16 Pct Recovery = 49% Analysis Date = 12/26/16 Pct Recovery = 49% Analysis Date = 12/21/16 Pct Recovery = 48% Analysis Date = 12/21/16 Pct Recovery = 48% Analysis Date = 12/17/16 Pct Recovery = 48% Analysis Date = 12/17/16 Pct Recovery = 48% Analysis Date = 12/12/16 Pct Recovery = 48% Analysis Date = 12/12/16 Pct Recovery = 48% Analysis Date = 12/07/16 Pct Recovery = 47% Analysis Date = 12/07/16 Pct Recovery = 47% Analysis Date = 12/03/16 Pct Recovery = 47% Analysis Date = 12/03/16 Pct Recovery = 47% Analysis Date = 11/28/16 Pct Recovery = 47% Analysis Date = 11/28/16 Pct Recovery = 47% Analysis Date = 11/23/16 Pct Recovery = 46% Analysis Date = 11/23/16 Pct Recovery = 46% Analysis Date = 11/19/16 Pct Recovery = 46% Analysis Date = 11/19/16 Pct Recovery = 46% Analysis Date = 11/14/16 Pct Recovery = 46% Analysis Date = 11/14/16 Pct Recovery = 46% Analysis Date = 11/09/16 Pct Recovery = 45% Analysis Date = 11/09/16 Pct Recovery = 45% Analysis Date = 11/05/16 Pct Recovery = 45% Analysis Date = 11/05/16 Pct Recovery = 45% Analysis Date = 10/31/16 Pct Recovery = 45% Analysis Date = 10/31/16 Pct Recovery = 45% Analysis Date = 10/26/16 Pct Recovery = 44% Analysis Date = 10/26/16 Pct Recovery = 44% Analysis Date = 10/22/16 Pct Recovery = 44% Analysis Date = 10/22/16 Pct Recovery = 44% Analysis Date = 10/17/16 Pct Recovery = 44% Analysis Date = 10/17/16 Pct Recovery = 44% Analysis Date = 10/12/16 Pct Recovery = 43% Analysis Date = 10/12/16 Pct Recovery = 43% Analysis Date = 10/08/16 Pct Recovery = 43% Analysis Date = 10/08/16 Pct Recovery = 43% Analysis Date = 10/03/16 Pct Recovery = 43% Analysis Date = 10/03/16 Pct Recovery = 43% Analysis Date = 09/28/16 Pct Recovery = 42% Analysis Date = 09/28/16 Pct Recovery = 42% Analysis Date = 09/24/16 Pct Recovery = 42% Analysis Date = 09/24/16 Pct Recovery = 42% Analysis Date = 09/19/16 Pct Recovery = 42% Analysis Date = 09/19/16 Pct Recovery = 42% Analysis Date = 09/14/16 Pct Recovery = 41% Analysis Date = 09/14/16 Pct Recovery = 41% Analysis Date = 09/09/16 Pct Recovery = 41% Analysis Date = 09/09/16 Pct Recovery = 41% Analysis Date = 09/05/16 Pct Recovery = 41% Analysis Date = 09/05/16 Pct Recovery = 41% Analysis Date = 08/31/16 Pct Recovery = 40% Analysis Date = 08/31/16 Pct Recovery = 40% Analysis Date = 08/26/16 Pct Recovery = 40% Analysis Date = 08/26/16 Pct Recovery = 40% Analysis Date = 08/22/16 Pct Recovery = 40% Analysis Date = 08/22/16 Pct Recovery = 40% Analysis Date = 08/17/16 Pct Recovery = 39% Analysis Date = 08/17/16 Pct Recovery = 39% Analysis Date = 08/12/16 Pct Recovery = 39% Analysis Date = 08/12/16 Pct Recovery = 39% Analysis Date = 08/08/16 Pct Recovery = 39% Analysis Date = 08/08/16 Pct Recovery = 39% Analysis Date = 08/03/16 Pct Recovery = 38% Analysis Date = 08/03/16 Pct Recovery = 38% Analysis Date = 07/29/16 Pct Recovery = 38% Analysis Date = 07/29/16 Pct Recovery = 38% Analysis Date = 07/25/16 Pct Recovery = 38% Analysis Date = 07/25/16 Pct Recovery = 38% Analysis Date = 07/20/16 Pct Recovery = 38% Analysis Date = 07/20/16 Pct Recovery = 38% Analysis Date = 07/15/16 Pct Recovery = 38% Analysis Date = 07/15/16 Pct Recovery = 38% Analysis Date = 07/11/16 Pct Recovery = 38% Analysis Date = 07/11/16 Pct Recovery = 38% Analysis Date = 07/06/16 Pct Recovery = 38% Analysis Date = 07/06/16 Pct Recovery = 38% Analysis Date = 07/01/16 Pct Recovery = 38% Analysis Date = 07/01/16 Pct Recovery = 38% Analysis Date = 06/27/16 Pct Recovery = 38% Analysis Date = 06/27/16 Pct Recovery = 38% Analysis Date = 06/22/16 Pct Recovery = 38% Analysis Date = 06/22/16 Pct Recovery = 38% Analysis Date = 06/17/16 Pct Recovery = 38% Analysis Date = 06/17/16 Pct Recovery = 38% Analysis Date = 06/13/16 Pct Recovery = 38% Analysis Date = 06/13/16 Pct Recovery = 38% Analysis Date = 06/08/16 Pct Recovery = 38% Analysis Date = 06/08/16 Pct Recovery = 38% Analysis Date = 06/03/16 Pct Recovery = 38% Analysis Date = 06/03/16 Pct Recovery = 38% Analysis Date = 05/30/16 Pct Recovery = 39% Analysis Date = 05/30/16 Pct Recovery = 39% Analysis Date = 05/25/16 Pct Recovery = 39% Analysis Date = 05/25/16 Pct Recovery = 39% Analysis Date = 05/20/16 Pct Recovery = 39% Analysis Date = 05/20/16 Pct Recovery = 39% Analysis Date = 05/15/16 Pct Recovery = 39% Analysis Date = 05/15/16 Pct Recovery = 39% Analysis Date = 05/11/16 Pct Recovery = 39% Analysis Date = 05/11/16 Pct Recovery = 39% Analysis Date = 05/06/16 Pct Recovery = 39% Analysis Date = 05/06/16 Pct Recovery = 39% Analysis Date = 05/01/16 Pct Recovery = 39% Analysis Date = 05/01/16 Pct Recovery = 39% Analysis Date = 04/27/16 Pct Recovery = 39% Analysis Date = 04/27/16 Pct Recovery = 39% Analysis Date = 04/22/16 Pct Recovery = 39% Analysis Date = 04/22/16 Pct Recovery = 39% Analysis Date = 04/17/16 Pct Recovery = 39% Analysis Date = 04/17/16 Pct Recovery = 39% Analysis Date = 04/13/16 Pct Recovery = 39% Analysis Date = 04/13/16 Pct Recovery = 39% Analysis Date = 04/08/16 Pct Recovery = 40% Analysis Date = 04/08/16 Pct Recovery = 40% Analysis Date = 04/03/16 Pct Recovery = 40% Analysis Date = 04/03/16 Pct Recovery = 40% Analysis Date = 03/30/16 Pct Recovery = 40% Analysis Date = 03/30/16 Pct Recovery = 40% Analysis Date = 03/25/16 Pct Recovery = 40% Analysis Date = 03/25/16 Pct Recovery = 40% Analysis Date = 03/20/16 Pct Recovery = 40% Analysis Date = 03/20/16 Pct Recovery = 40% Analysis Date = 03/16/16 Pct Recovery = 40% Analysis Date = 03/16/16 Pct Recovery = 40% Analysis Date = 03/11/16 Pct Recovery = 40% Analysis Date = 03/11/16 Pct Recovery = 40% Analysis Date = 03/06/16 Pct Recovery = 40% Analysis Date = 03/06/16 Pct Recovery = 40% Analysis Date = 03/02/16 Pct Recovery = 40% Analysis Date = 03/02/16 Pct Recovery = 40% Analysis Date = 02/26/16 Pct Recovery = 40% Analysis Date = 02/26/16 Pct Recovery = 40% Analysis Date = 02/21/16 Pct Recovery = 40% Analysis Date = 02/21/16 Pct Recovery = 40% Analysis Date = 02/17/16 Pct Recovery = 41% Analysis Date = 02/17/16 Pct Recovery = 41% Analysis Date = 02/12/16 Pct Recovery = 41% Analysis Date = 02/12/16 Pct Recovery = 41% Analysis Date = 02/07/16 Pct Recovery = 41% Analysis Date = 02/07/16 Pct Recovery = 41% Analysis Date = 02/03/16 Pct Recovery = 41% Analysis Date = 02/03/16 Pct Recovery = 41% Analysis Date = 01/29/16 Pct Recovery = 41% Analysis Date = 01/29/16 Pct Recovery = 41% Analysis Date = 01/24/16 Pct Recovery = 41% Analysis Date = 01/24/16 Pct Recovery = 41% Analysis Date = 01/19/16 Pct Recovery = 41% Analysis Date = 01/19/16 Pct Recovery = 41% Analysis Date = 01/15/16 Pct Recovery = 41% Analysis Date = 01/15/16 Pct Recovery = 41% Analysis Date = 01/10/16 Pct Recovery = 41% Analysis Date = 01/10/16 Pct Recovery = 41% Analysis Date = 01/05/16 Pct Recovery = 41% Analysis Date = 01/05/16 Pct Recovery = 41% Analysis Date = 01/01/16 Pct Recovery = 41% Analysis Date = 01/01/16 Pct Recovery = 41% Analysis Date = 12/27/15 Pct Recovery = 42% Analysis Date = 12/27/15 Pct Recovery = 42% Analysis Date = 12/22/15 Pct Recovery = 42% Analysis Date = 12/22/15 Pct Recovery = 42% Analysis Date = 12/18/15 Pct Recovery = 42% Analysis Date = 12/18/15 Pct Recovery = 42% Analysis Date = 12/13/15 Pct Recovery = 42% Analysis Date = 12/13/15 Pct Recovery = 42% Analysis Date = 12/08/15 Pct Recovery = 42% Analysis Date = 12/08/15 Pct Recovery = 42% Analysis Date = 12/04/15 Pct Recovery = 42% Analysis Date = 12/04/15 Pct Recovery = 42% Analysis Date = 11/29/15 Pct Recovery = 42% Analysis Date = 11/29/15 Pct Recovery = 42% Analysis Date = 11/24/15 Pct Recovery = 42% Analysis Date = 11/24/15 Pct Recovery = 42% Analysis Date = 11/20/15 Pct Recovery = 42% Analysis Date = 11/20/15 Pct Recovery = 42% Analysis Date = 11/15/15 Pct Recovery = 42% Analysis Date = 11/15/15 Pct Recovery = 42% Analysis Date = 11/10/15 Pct Recovery = 42% Analysis Date = 11/10/15 Pct Recovery = 42% Analysis Date = 11/06/15 Pct Recovery = 42% Analysis Date = 11/06/15 Pct Recovery = 42% Analysis Date = 11/01/15 Pct Recovery = 43% Analysis Date = 11/01/15 Pct Recovery = 43% Analysis Date = 10/27/15 Pct Recovery = 43% Analysis Date = 10/27/15 Pct Recovery = 43% Analysis Date = 10/23/15 Pct Recovery = 43% Analysis Date = 10/23/15 Pct Recovery = 43% Analysis Date = 10/18/15 Pct Recovery = 43% Analysis Date = 10/18/15 Pct Recovery = 43% Analysis Date = 10/13/15 Pct Recovery = 43% Analysis Date = 10/13/15 Pct Recovery = 43% Analysis Date = 10/09/15 Pct Recovery = 43% Analysis Date = 10/09/15 Pct Recovery = 43% Analysis Date = 10/04/15 Pct Recovery = 43% Analysis Date = 10/04/15 Pct Recovery = 43% Analysis Date = 09/29/15 Pct Recovery = 43% Analysis Date = 09/29/15 Pct Recovery = 43% Analysis Date = 09/24/15 Pct Recovery = 43% Analysis Date = 09/24/15 Pct Recovery = 43% Analysis Date = 09/20/15 Pct Recovery = 43% Analysis Date = 09/20/15 Pct Recovery = 43% Analysis Date = 09/15/15 Pct Recovery = 43% Analysis Date = 09/15/15 Pct Recovery = 43% Analysis Date = 09/10/15 Pct Recovery = 44% Analysis Date = 09/10/15 Pct Recovery = 44% Analysis Date = 09/06/15 Pct Recovery = 44% Analysis Date = 09/06/15 Pct Recovery = 44% Analysis Date = 09/01/15 Pct Recovery = 44% Analysis Date = 09/01/15 Pct Recovery = 44% Analysis Date = 08/27/15 Pct Recovery = 44% Analysis Date = 08/27/15 Pct Recovery = 44% Analysis Date = 08/23/15 Pct Recovery = 44% Analysis Date = 08/23/15 Pct Recovery = 44% Analysis Date = 08/18/15 Pct Recovery = 44% Analysis Date = 08/18/15 Pct Recovery = 44% Analysis Date = 08/13/15 Pct Recovery = 44% Analysis Date = 08/13/15 Pct Recovery = 44% Analysis Date = 08/09/15 Pct Recovery = 44% Analysis Date = 08/09/15 Pct Recovery = 44% Analysis Date = 08/04/15 Pct Recovery = 44% Analysis Date = 08/04/15 Pct Recovery = 44% Analysis Date = 07/30/15 Pct Recovery = 44% Analysis Date = 07/30/15 Pct Recovery = 44% Analysis Date = 07/26/15 Pct Recovery = 44% Analysis Date = 07/26/15 Pct Recovery = 44% Analysis Date = 07/21/15 Pct Recovery = 45% Analysis Date = 07/21/15 Pct Recovery = 45% Analysis Date = 07/16/15 Pct Recovery = 45% Analysis Date = 07/16/15 Pct Recovery = 45% Analysis Date = 07/12/15 Pct Recovery = 45% Analysis Date = 07/12/15 Pct Recovery = 45% Analysis Date = 07/07/15 Pct Recovery = 45% Analysis Date = 07/07/15 Pct Recovery = 45% Analysis Date = 07/02/15 Pct Recovery = 45% Analysis Date = 07/02/15 Pct Recovery = 45% Analysis Date = 06/28/15 Pct Recovery = 45% Analysis Date = 06/28/15 Pct Recovery = 45% Analysis Date = 06/23/15 Pct Recovery = 45% Analysis Date = 06/23/15 Pct Recovery = 45% Analysis Date = 06/18/15 Pct Recovery = 45% Analysis Date = 06/18/15 Pct Recovery = 45% Analysis Date = 06/14/15 Pct Recovery = 45% Analysis Date = 06/14/15 Pct Recovery = 45% Analysis Date = 06/09/15 Pct Recovery = 45% Analysis Date = 06/09/15 Pct Recovery = 45% Analysis Date = 06/04/15 Pct Recovery = 45% Analysis Date = 06/04/15 Pct Recovery = 45% Analysis Date = 05/30/15 Pct Recovery = 46% Analysis Date = 05/30/15 Pct Recovery = 46% Analysis Date = 05/26/15 Pct Recovery = 46% Analysis Date = 05/26/15 Pct Recovery = 46% Analysis Date = 05/21/15 Pct Recovery = 46% Analysis Date = 05/21/15 Pct Recovery = 46% Analysis Date = 05/16/15 Pct Recovery = 46% Analysis Date = 05/16/15 Pct Recovery = 46% Analysis Date = 05/12/15 Pct Recovery = 46% Analysis Date = 05/12/15 Pct Recovery = 46% Analysis Date = 05/07/15 Pct Recovery = 46% Analysis Date = 05/07/15 Pct Recovery = 46% Analysis Date = 05/02/15 Pct Recovery = 46% Analysis Date = 05/02/15 Pct Recovery = 46% Analysis Date = 04/28/15 Pct Recovery = 46% Analysis Date = 04/28/15 Pct Recovery = 46% Analysis Date = 04/23/15 Pct Recovery = 46% Analysis Date = 04/23/15 Pct Recovery = 46% Analysis Date = 04/18/15 Pct Recovery = 46% Analysis Date = 04/18/15 Pct Recovery = 46% Analysis Date = 04/14/15 Pct Recovery = 46% Analysis Date = 04/14/15 Pct Recovery = 46% Analysis Date = 04/09/15 Pct Recovery = 47% Analysis Date = 04/09/15 Pct Recovery = 47% Analysis Date = 04/04/15 Pct Recovery = 47% Analysis Date = 04/04/15 Pct Recovery = 47% Analysis Date = 03/31/15 Pct Recovery = 47% Analysis Date = 03/31/15 Pct Recovery = 47% Analysis Date = 03/26/15 Pct Recovery = 47% Analysis Date = 03/26/15 Pct Recovery = 47% Analysis Date = 03/21/15 Pct Recovery = 47% Analysis Date = 03/21/15 Pct Recovery = 47% Analysis Date = 03/17/15 Pct Recovery = 47% Analysis Date = 03/17/15 Pct Recovery = 47% Analysis Date = 03/12/15 Pct Recovery = 47% Analysis Date = 03/12/15 Pct Recovery = 47% Analysis Date = 03/07/15 Pct Recovery = 47% Analysis Date = 03/07/15 Pct Recovery = 47% Analysis Date = 03/03/15 Pct Recovery = 47% Analysis Date = 03/03/15 Pct Recovery = 47% Analysis Date = 02/26/15 Pct Recovery = 47% Analysis Date = 02/26/15 Pct Recovery = 47% Analysis Date = 02/21/15 Pct Recovery = 46% Analysis Date = 02/21/15 Pct Recovery = 46% Analysis Date = 02/17/15 Pct Recovery = 46% Analysis Date = 02/17/15 Pct Recovery = 46% Analysis Date = 02/12/15 Pct Recovery = 46% Analysis Date = 02/12/15 Pct Recovery = 46% Analysis Date = 02/07/15 Pct Recovery = 46% Analysis Date = 02/07/15 Pct Recovery = 46% Analysis Date = 02/02/15 Pct Recovery = 46% Analysis Date = 02/02/15 Pct Recovery = 46% Analysis Date = 01/29/15 Pct Recovery = 46% Analysis Date = 01/29/15 Pct Recovery = 46% Analysis Date = 01/24/15 Pct Recovery = 45% Analysis Date = 01/24/15 Pct Recovery = 45% Analysis Date = 01/19/15 Pct Recovery = 45% Analysis Date = 01/19/15 Pct Recovery = 45% Analysis Date = 01/15/15 Pct Recovery = 45% Analysis Date = 01/15/15 Pct Recovery = 45% Analysis Date = 01/10/15 Pct Recovery = 45% Analysis Date = 01/10/15 Pct Recovery = 45% Analysis Date = 01/05/15 Pct Recovery = 45% Analysis Date = 01/05/15 Pct Recovery = 45% Analysis Date = 01/01/15 Pct Recovery = 44% Analysis Date = 01/01/15 Pct Recovery = 44% Analysis Date = 12/27/14 Pct Recovery = 44% Analysis Date = 12/27/14 Pct Recovery = 44% Analysis Date = 12/22/14 Pct Recovery = 44% Analysis Date = 12/22/14 Pct Recovery = 44% Analysis Date = 12/18/14 Pct Recovery = 44% Analysis Date = 12/18/14 Pct Recovery = 44% Analysis Date = 12/13/14 Pct Recovery = 44% Analysis Date = 12/13/14 Pct Recovery = 44% Analysis Date = 12/08/14 Pct Recovery = 43% Analysis Date = 12/08/14 Pct Recovery = 43% Analysis Date = 12/04/14 Pct Recovery = 43% Analysis Date = 12/04/14 Pct Recovery = 43% Analysis Date = 11/29/14 Pct Recovery = 43% Analysis Date = 11/29/14 Pct Recovery = 43% Analysis Date = 11/24/14 Pct Recovery = 43% Analysis Date = 11/24/14 Pct Recovery = 43% Analysis Date = 11/20/14 Pct Recovery = 43% Analysis Date = 11/20/14 Pct Recovery = 43% Analysis Date = 11/15/14 Pct Recovery = 42% Analysis Date = 11/15/14 Pct Recovery = 42% Analysis Date = 11/10/14 Pct Recovery = 42% Analysis Date = 11/10/14 Pct Recovery = 42% Analysis Date = 11/06/14 Pct Recovery = 42% Analysis Date = 11/06/14 Pct Recovery = 42% Analysis Date = 11/01/14 Pct Recovery = 42% Analysis Date = 11/01/14 Pct Recovery = 42% Analysis Date = 10/27/14 Pct Recovery = 42% Analysis Date = 10/27/14 Pct Recovery = 42% Analysis Date = 10/23/14 Pct Recovery = 41% Analysis Date = 10/23/14 Pct Recovery = 41% Analysis Date = 10/18/14 Pct Recovery = 41% Analysis Date = 10/18/14 Pct Recovery = 41% Analysis Date = 10/13/14 Pct Recovery = 41% Analysis Date = 10/13/14 Pct Recovery = 41% Analysis Date = 10/08/14 Pct Recovery = 41% Analysis Date = 10/08/14 Pct Recovery = 41% Analysis Date = 10/04/14 Pct Recovery = 41% Analysis Date = 10/04/14 Pct Recovery = 41% Analysis Date = 09/29/14 Pct Recovery = 40% Analysis Date = 09/29/14 Pct Recovery = 40% Analysis Date = 09/24/14 Pct Recovery = 40% Analysis Date = 09/24/14 Pct Recovery = 40% Analysis Date = 09/20/14 Pct Recovery = 40% Analysis Date = 09/20/14 Pct Recovery = 40% Analysis Date = 09/15/14 Pct Recovery = 40% Analysis Date = 09/15/14 Pct Recovery = 40% Analysis Date = 09/10/14 Pct Recovery = 39% Analysis Date = 09/10/14 Pct Recovery = 39% Analysis Date = 09/06/14 Pct Recovery = 39% Analysis Date = 09/06/14 Pct Recovery = 39% Analysis Date = 09/01/14 Pct Recovery = 39% Analysis Date = 09/01/14 Pct Recovery = 39% Analysis Date = 08/27/14 Pct Recovery = 39% Analysis Date = 08/27/14 Pct Recovery = 39% Analysis Date = 08/23/14 Pct Recovery = 39% Analysis Date = 08/23/14 Pct Recovery = 39% Analysis Date = 08/18/14 Pct Recovery = 38% Analysis Date = 08/18/14 Pct Recovery = 38% Analysis Date = 08/13/14 Pct Recovery = 38% Analysis Date = 08/13/14 Pct Recovery = 38% Analysis Date = 08/09/14 Pct Recovery = 38% Analysis Date = 08/09/14 Pct Recovery = 38% Analysis Date = 08/04/14 Pct Recovery = 38% Analysis Date = 08/04/14 Pct Recovery = 38% Analysis Date = 07/30/14 Pct Recovery = 37% Analysis Date = 07/30/14 Pct Recovery = 37% Analysis Date = 07/26/14 Pct Recovery = 37% Analysis Date = 07/26/14 Pct Recovery = 37% Analysis Date = 07/21/14 Pct Recovery = 37% Analysis Date = 07/21/14 Pct Recovery = 37% Analysis Date = 07/16/14 Pct Recovery = 37% Analysis Date = 07/16/14 Pct Recovery = 37% Analysis Date = 07/12/14 Pct Recovery = 36% Analysis Date = 07/12/14 Pct Recovery = 36% Analysis Date = 07/07/14 Pct Recovery = 36% Analysis Date = 07/07/14 Pct Recovery = 36% Analysis Date = 07/02/14 Pct Recovery = 36% Analysis Date = 07/02/14 Pct Recovery = 36% Analysis Date = 06/28/14 Pct Recovery = 36% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
CHLORPHENIRAMINE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 12 46% 15% 43% 11%
>= Reporting Level 32 42% 12% 40% 12%
Total 44 43% 12% 41% 12%

Sample Statistics
CHLORPHENIRAMINE

Characteristic N % % Basis
Plotted 44 69% Spiked
Estimated Values 25 39% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 64 .  
False Negatives 20 31% 20 out of 64
Not Spiked 51 .  
False Positives 0 0% 0 out of 51

BQS OBSP Determination:
CIMETIDINE
METHOD: 2440 , TESTIDCODE: 67442LCM56
Open Data Set

Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 44% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 36% Analysis Date = 11/05/15 SpikeMix = ERA 0406-15-08: 80 µl & Abs 052215: 80 µl Pct Recovery = 14% Analysis Date = 01/17/16 SpikeMix = ERA 0406-15-09: 80 µl & ERA 0406-15-07A: 80 µl Pct Recovery = 40% Analysis Date = 11/24/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 30% Analysis Date = 11/18/16 SpikeMix = ERA 04281604: 80 µl & ERA 04281603: 80 µl Pct Recovery = 52% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & ERA 04281604: 80 µl Pct Recovery = 49% Analysis Date = 09/24/16 SpikeMix = Crescent EN160610015: 80 µl & Abs 061416: 80 µl Pct Recovery = 15% Analysis Date = 09/24/16 SpikeMix = Abs 061416: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 16% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 12% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 16% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-04: 15 µl & Abs 041814: 15 µl Pct Recovery = 60% Analysis Date = 10/25/14 SpikeMix = Abs 041614: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 52% Analysis Date = 10/11/14 SpikeMix = ERA 0318-14-02: 60 µl & ERA 0319-14-04: 60 µl Pct Recovery = 37% Analysis Date = 08/28/14 SpikeMix = ERA 0319-14-04: 60 µl & ERA 0319-14-05: 60 µl Pct Recovery = 49% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-08: 40 µl & ERA 0406-15-09: 40 µl Pct Recovery = 15% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 38% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 35% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 25% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 30% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 43% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 50% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 98% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 100% Analysis Date = 04/30/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 78% Analysis Date = 04/10/15 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 75% Analysis Date = 02/10/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 19% Analysis Date = 12/07/14 SpikeMix = ERA 0318-14-02: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 78% Analysis Date = 10/11/14 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 69% Analysis Date = 10/10/14 SpikeMix = Abs 041714: 30 µl & Abs 041814: 30 µl Pct Recovery = 50% Analysis Date = 09/12/14 SpikeMix = Abs 041614: 30 µl & ERA 0319-14-04: 30 µl Pct Recovery = 64% Analysis Date = 08/16/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 85% Analysis Date = 07/13/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 82% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 69% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 39% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-08: 20 µl & ERA 0406-15-09: 20 µl Pct Recovery = 50% Analysis Date = 04/09/16 SpikeMix = Abs 051315: 10 µl & ERA 0406-15-09: 10 µl Pct Recovery = 68% Analysis Date = 01/04/17 Pct Recovery = 35% Analysis Date = 12/31/16 Pct Recovery = 35% Analysis Date = 12/31/16 Pct Recovery = 35% Analysis Date = 12/26/16 Pct Recovery = 35% Analysis Date = 12/26/16 Pct Recovery = 35% Analysis Date = 12/22/16 Pct Recovery = 36% Analysis Date = 12/22/16 Pct Recovery = 36% Analysis Date = 12/17/16 Pct Recovery = 36% Analysis Date = 12/17/16 Pct Recovery = 36% Analysis Date = 12/13/16 Pct Recovery = 37% Analysis Date = 12/13/16 Pct Recovery = 37% Analysis Date = 12/08/16 Pct Recovery = 37% Analysis Date = 12/08/16 Pct Recovery = 37% Analysis Date = 12/04/16 Pct Recovery = 37% Analysis Date = 12/04/16 Pct Recovery = 37% Analysis Date = 11/29/16 Pct Recovery = 38% Analysis Date = 11/29/16 Pct Recovery = 38% Analysis Date = 11/25/16 Pct Recovery = 38% Analysis Date = 11/25/16 Pct Recovery = 38% Analysis Date = 11/20/16 Pct Recovery = 38% Analysis Date = 11/20/16 Pct Recovery = 38% Analysis Date = 11/16/16 Pct Recovery = 39% Analysis Date = 11/16/16 Pct Recovery = 39% Analysis Date = 11/11/16 Pct Recovery = 39% Analysis Date = 11/11/16 Pct Recovery = 39% Analysis Date = 11/07/16 Pct Recovery = 39% Analysis Date = 11/07/16 Pct Recovery = 39% Analysis Date = 11/02/16 Pct Recovery = 40% Analysis Date = 11/02/16 Pct Recovery = 40% Analysis Date = 10/28/16 Pct Recovery = 40% Analysis Date = 10/28/16 Pct Recovery = 40% Analysis Date = 10/24/16 Pct Recovery = 40% Analysis Date = 10/24/16 Pct Recovery = 40% Analysis Date = 10/19/16 Pct Recovery = 41% Analysis Date = 10/19/16 Pct Recovery = 41% Analysis Date = 10/15/16 Pct Recovery = 41% Analysis Date = 10/15/16 Pct Recovery = 41% Analysis Date = 10/10/16 Pct Recovery = 41% Analysis Date = 10/10/16 Pct Recovery = 41% Analysis Date = 10/06/16 Pct Recovery = 42% Analysis Date = 10/06/16 Pct Recovery = 42% Analysis Date = 10/01/16 Pct Recovery = 42% Analysis Date = 10/01/16 Pct Recovery = 42% Analysis Date = 09/27/16 Pct Recovery = 42% Analysis Date = 09/27/16 Pct Recovery = 42% Analysis Date = 09/22/16 Pct Recovery = 43% Analysis Date = 09/22/16 Pct Recovery = 43% Analysis Date = 09/18/16 Pct Recovery = 43% Analysis Date = 09/18/16 Pct Recovery = 43% Analysis Date = 09/13/16 Pct Recovery = 43% Analysis Date = 09/13/16 Pct Recovery = 43% Analysis Date = 09/09/16 Pct Recovery = 44% Analysis Date = 09/09/16 Pct Recovery = 44% Analysis Date = 09/04/16 Pct Recovery = 44% Analysis Date = 09/04/16 Pct Recovery = 44% Analysis Date = 08/31/16 Pct Recovery = 44% Analysis Date = 08/31/16 Pct Recovery = 44% Analysis Date = 08/26/16 Pct Recovery = 45% Analysis Date = 08/26/16 Pct Recovery = 45% Analysis Date = 08/21/16 Pct Recovery = 45% Analysis Date = 08/21/16 Pct Recovery = 45% Analysis Date = 08/17/16 Pct Recovery = 45% Analysis Date = 08/17/16 Pct Recovery = 45% Analysis Date = 08/12/16 Pct Recovery = 46% Analysis Date = 08/12/16 Pct Recovery = 46% Analysis Date = 08/08/16 Pct Recovery = 46% Analysis Date = 08/08/16 Pct Recovery = 46% Analysis Date = 08/03/16 Pct Recovery = 46% Analysis Date = 08/03/16 Pct Recovery = 46% Analysis Date = 07/30/16 Pct Recovery = 47% Analysis Date = 07/30/16 Pct Recovery = 47% Analysis Date = 07/25/16 Pct Recovery = 47% Analysis Date = 07/25/16 Pct Recovery = 47% Analysis Date = 07/21/16 Pct Recovery = 47% Analysis Date = 07/21/16 Pct Recovery = 47% Analysis Date = 07/16/16 Pct Recovery = 47% Analysis Date = 07/16/16 Pct Recovery = 47% Analysis Date = 07/12/16 Pct Recovery = 47% Analysis Date = 07/12/16 Pct Recovery = 47% Analysis Date = 07/07/16 Pct Recovery = 47% Analysis Date = 07/07/16 Pct Recovery = 47% Analysis Date = 07/03/16 Pct Recovery = 47% Analysis Date = 07/03/16 Pct Recovery = 47% Analysis Date = 06/28/16 Pct Recovery = 47% Analysis Date = 06/28/16 Pct Recovery = 47% Analysis Date = 06/23/16 Pct Recovery = 46% Analysis Date = 06/23/16 Pct Recovery = 46% Analysis Date = 06/19/16 Pct Recovery = 46% Analysis Date = 06/19/16 Pct Recovery = 46% Analysis Date = 06/14/16 Pct Recovery = 46% Analysis Date = 06/14/16 Pct Recovery = 46% Analysis Date = 06/10/16 Pct Recovery = 46% Analysis Date = 06/10/16 Pct Recovery = 46% Analysis Date = 06/05/16 Pct Recovery = 46% Analysis Date = 06/05/16 Pct Recovery = 46% Analysis Date = 06/01/16 Pct Recovery = 46% Analysis Date = 06/01/16 Pct Recovery = 46% Analysis Date = 05/27/16 Pct Recovery = 46% Analysis Date = 05/27/16 Pct Recovery = 46% Analysis Date = 05/23/16 Pct Recovery = 45% Analysis Date = 05/23/16 Pct Recovery = 45% Analysis Date = 05/18/16 Pct Recovery = 45% Analysis Date = 05/18/16 Pct Recovery = 45% Analysis Date = 05/14/16 Pct Recovery = 45% Analysis Date = 05/14/16 Pct Recovery = 45% Analysis Date = 05/09/16 Pct Recovery = 45% Analysis Date = 05/09/16 Pct Recovery = 45% Analysis Date = 05/05/16 Pct Recovery = 45% Analysis Date = 05/05/16 Pct Recovery = 45% Analysis Date = 04/30/16 Pct Recovery = 45% Analysis Date = 04/30/16 Pct Recovery = 45% Analysis Date = 04/26/16 Pct Recovery = 44% Analysis Date = 04/26/16 Pct Recovery = 44% Analysis Date = 04/21/16 Pct Recovery = 44% Analysis Date = 04/21/16 Pct Recovery = 44% Analysis Date = 04/16/16 Pct Recovery = 44% Analysis Date = 04/16/16 Pct Recovery = 44% Analysis Date = 04/12/16 Pct Recovery = 44% Analysis Date = 04/12/16 Pct Recovery = 44% Analysis Date = 04/07/16 Pct Recovery = 44% Analysis Date = 04/07/16 Pct Recovery = 44% Analysis Date = 04/03/16 Pct Recovery = 44% Analysis Date = 04/03/16 Pct Recovery = 44% Analysis Date = 03/29/16 Pct Recovery = 44% Analysis Date = 03/29/16 Pct Recovery = 44% Analysis Date = 03/25/16 Pct Recovery = 43% Analysis Date = 03/25/16 Pct Recovery = 43% Analysis Date = 03/20/16 Pct Recovery = 43% Analysis Date = 03/20/16 Pct Recovery = 43% Analysis Date = 03/16/16 Pct Recovery = 43% Analysis Date = 03/16/16 Pct Recovery = 43% Analysis Date = 03/11/16 Pct Recovery = 43% Analysis Date = 03/11/16 Pct Recovery = 43% Analysis Date = 03/07/16 Pct Recovery = 43% Analysis Date = 03/07/16 Pct Recovery = 43% Analysis Date = 03/02/16 Pct Recovery = 43% Analysis Date = 03/02/16 Pct Recovery = 43% Analysis Date = 02/27/16 Pct Recovery = 43% Analysis Date = 02/27/16 Pct Recovery = 43% Analysis Date = 02/22/16 Pct Recovery = 43% Analysis Date = 02/22/16 Pct Recovery = 43% Analysis Date = 02/18/16 Pct Recovery = 43% Analysis Date = 02/18/16 Pct Recovery = 43% Analysis Date = 02/13/16 Pct Recovery = 43% Analysis Date = 02/13/16 Pct Recovery = 43% Analysis Date = 02/08/16 Pct Recovery = 43% Analysis Date = 02/08/16 Pct Recovery = 43% Analysis Date = 02/04/16 Pct Recovery = 43% Analysis Date = 02/04/16 Pct Recovery = 43% Analysis Date = 01/30/16 Pct Recovery = 43% Analysis Date = 01/30/16 Pct Recovery = 43% Analysis Date = 01/26/16 Pct Recovery = 43% Analysis Date = 01/26/16 Pct Recovery = 43% Analysis Date = 01/21/16 Pct Recovery = 43% Analysis Date = 01/21/16 Pct Recovery = 43% Analysis Date = 01/17/16 Pct Recovery = 43% Analysis Date = 01/17/16 Pct Recovery = 43% Analysis Date = 01/12/16 Pct Recovery = 43% Analysis Date = 01/12/16 Pct Recovery = 43% Analysis Date = 01/08/16 Pct Recovery = 43% Analysis Date = 01/08/16 Pct Recovery = 43% Analysis Date = 01/03/16 Pct Recovery = 43% Analysis Date = 01/03/16 Pct Recovery = 43% Analysis Date = 12/30/15 Pct Recovery = 43% Analysis Date = 12/30/15 Pct Recovery = 43% Analysis Date = 12/25/15 Pct Recovery = 44% Analysis Date = 12/25/15 Pct Recovery = 44% Analysis Date = 12/21/15 Pct Recovery = 44% Analysis Date = 12/21/15 Pct Recovery = 44% Analysis Date = 12/16/15 Pct Recovery = 44% Analysis Date = 12/16/15 Pct Recovery = 44% Analysis Date = 12/11/15 Pct Recovery = 44% Analysis Date = 12/11/15 Pct Recovery = 44% Analysis Date = 12/07/15 Pct Recovery = 44% Analysis Date = 12/07/15 Pct Recovery = 44% Analysis Date = 12/02/15 Pct Recovery = 44% Analysis Date = 12/02/15 Pct Recovery = 44% Analysis Date = 11/28/15 Pct Recovery = 44% Analysis Date = 11/28/15 Pct Recovery = 44% Analysis Date = 11/23/15 Pct Recovery = 44% Analysis Date = 11/23/15 Pct Recovery = 44% Analysis Date = 11/19/15 Pct Recovery = 44% Analysis Date = 11/19/15 Pct Recovery = 44% Analysis Date = 11/14/15 Pct Recovery = 44% Analysis Date = 11/14/15 Pct Recovery = 44% Analysis Date = 11/10/15 Pct Recovery = 44% Analysis Date = 11/10/15 Pct Recovery = 44% Analysis Date = 11/05/15 Pct Recovery = 44% Analysis Date = 11/05/15 Pct Recovery = 44% Analysis Date = 11/01/15 Pct Recovery = 44% Analysis Date = 11/01/15 Pct Recovery = 44% Analysis Date = 10/27/15 Pct Recovery = 44% Analysis Date = 10/27/15 Pct Recovery = 44% Analysis Date = 10/23/15 Pct Recovery = 45% Analysis Date = 10/23/15 Pct Recovery = 45% Analysis Date = 10/18/15 Pct Recovery = 45% Analysis Date = 10/18/15 Pct Recovery = 45% Analysis Date = 10/14/15 Pct Recovery = 45% Analysis Date = 10/14/15 Pct Recovery = 45% Analysis Date = 10/09/15 Pct Recovery = 45% Analysis Date = 10/09/15 Pct Recovery = 45% Analysis Date = 10/04/15 Pct Recovery = 45% Analysis Date = 10/04/15 Pct Recovery = 45% Analysis Date = 09/30/15 Pct Recovery = 45% Analysis Date = 09/30/15 Pct Recovery = 45% Analysis Date = 09/25/15 Pct Recovery = 45% Analysis Date = 09/25/15 Pct Recovery = 45% Analysis Date = 09/21/15 Pct Recovery = 46% Analysis Date = 09/21/15 Pct Recovery = 46% Analysis Date = 09/16/15 Pct Recovery = 46% Analysis Date = 09/16/15 Pct Recovery = 46% Analysis Date = 09/12/15 Pct Recovery = 46% Analysis Date = 09/12/15 Pct Recovery = 46% Analysis Date = 09/07/15 Pct Recovery = 46% Analysis Date = 09/07/15 Pct Recovery = 46% Analysis Date = 09/03/15 Pct Recovery = 46% Analysis Date = 09/03/15 Pct Recovery = 46% Analysis Date = 08/29/15 Pct Recovery = 46% Analysis Date = 08/29/15 Pct Recovery = 46% Analysis Date = 08/25/15 Pct Recovery = 46% Analysis Date = 08/25/15 Pct Recovery = 46% Analysis Date = 08/20/15 Pct Recovery = 46% Analysis Date = 08/20/15 Pct Recovery = 46% Analysis Date = 08/16/15 Pct Recovery = 47% Analysis Date = 08/16/15 Pct Recovery = 47% Analysis Date = 08/11/15 Pct Recovery = 47% Analysis Date = 08/11/15 Pct Recovery = 47% Analysis Date = 08/07/15 Pct Recovery = 47% Analysis Date = 08/07/15 Pct Recovery = 47% Analysis Date = 08/02/15 Pct Recovery = 47% Analysis Date = 08/02/15 Pct Recovery = 47% Analysis Date = 07/28/15 Pct Recovery = 47% Analysis Date = 07/28/15 Pct Recovery = 47% Analysis Date = 07/24/15 Pct Recovery = 47% Analysis Date = 07/24/15 Pct Recovery = 47% Analysis Date = 07/19/15 Pct Recovery = 47% Analysis Date = 07/19/15 Pct Recovery = 47% Analysis Date = 07/15/15 Pct Recovery = 48% Analysis Date = 07/15/15 Pct Recovery = 48% Analysis Date = 07/10/15 Pct Recovery = 48% Analysis Date = 07/10/15 Pct Recovery = 48% Analysis Date = 07/06/15 Pct Recovery = 48% Analysis Date = 07/06/15 Pct Recovery = 48% Analysis Date = 07/01/15 Pct Recovery = 48% Analysis Date = 07/01/15 Pct Recovery = 48% Analysis Date = 06/27/15 Pct Recovery = 48% Analysis Date = 06/27/15 Pct Recovery = 48% Analysis Date = 06/22/15 Pct Recovery = 48% Analysis Date = 06/22/15 Pct Recovery = 48% Analysis Date = 06/18/15 Pct Recovery = 48% Analysis Date = 06/18/15 Pct Recovery = 48% Analysis Date = 06/13/15 Pct Recovery = 49% Analysis Date = 06/13/15 Pct Recovery = 49% Analysis Date = 06/09/15 Pct Recovery = 49% Analysis Date = 06/09/15 Pct Recovery = 49% Analysis Date = 06/04/15 Pct Recovery = 49% Analysis Date = 06/04/15 Pct Recovery = 49% Analysis Date = 05/30/15 Pct Recovery = 49% Analysis Date = 05/30/15 Pct Recovery = 49% Analysis Date = 05/26/15 Pct Recovery = 49% Analysis Date = 05/26/15 Pct Recovery = 49% Analysis Date = 05/21/15 Pct Recovery = 49% Analysis Date = 05/21/15 Pct Recovery = 49% Analysis Date = 05/17/15 Pct Recovery = 49% Analysis Date = 05/17/15 Pct Recovery = 49% Analysis Date = 05/12/15 Pct Recovery = 50% Analysis Date = 05/12/15 Pct Recovery = 50% Analysis Date = 05/08/15 Pct Recovery = 50% Analysis Date = 05/08/15 Pct Recovery = 50% Analysis Date = 05/03/15 Pct Recovery = 50% Analysis Date = 05/03/15 Pct Recovery = 50% Analysis Date = 04/29/15 Pct Recovery = 50% Analysis Date = 04/29/15 Pct Recovery = 50% Analysis Date = 04/24/15 Pct Recovery = 50% Analysis Date = 04/24/15 Pct Recovery = 50% Analysis Date = 04/20/15 Pct Recovery = 51% Analysis Date = 04/20/15 Pct Recovery = 51% Analysis Date = 04/15/15 Pct Recovery = 51% Analysis Date = 04/15/15 Pct Recovery = 51% Analysis Date = 04/11/15 Pct Recovery = 51% Analysis Date = 04/11/15 Pct Recovery = 51% Analysis Date = 04/06/15 Pct Recovery = 51% Analysis Date = 04/06/15 Pct Recovery = 51% Analysis Date = 04/02/15 Pct Recovery = 52% Analysis Date = 04/02/15 Pct Recovery = 52% Analysis Date = 03/28/15 Pct Recovery = 52% Analysis Date = 03/28/15 Pct Recovery = 52% Analysis Date = 03/23/15 Pct Recovery = 52% Analysis Date = 03/23/15 Pct Recovery = 52% Analysis Date = 03/19/15 Pct Recovery = 52% Analysis Date = 03/19/15 Pct Recovery = 52% Analysis Date = 03/14/15 Pct Recovery = 53% Analysis Date = 03/14/15 Pct Recovery = 53% Analysis Date = 03/10/15 Pct Recovery = 53% Analysis Date = 03/10/15 Pct Recovery = 53% Analysis Date = 03/05/15 Pct Recovery = 53% Analysis Date = 03/05/15 Pct Recovery = 53% Analysis Date = 03/01/15 Pct Recovery = 54% Analysis Date = 03/01/15 Pct Recovery = 54% Analysis Date = 02/24/15 Pct Recovery = 54% Analysis Date = 02/24/15 Pct Recovery = 54% Analysis Date = 02/20/15 Pct Recovery = 54% Analysis Date = 02/20/15 Pct Recovery = 54% Analysis Date = 02/15/15 Pct Recovery = 54% Analysis Date = 02/15/15 Pct Recovery = 54% Analysis Date = 02/11/15 Pct Recovery = 55% Analysis Date = 02/11/15 Pct Recovery = 55% Analysis Date = 02/06/15 Pct Recovery = 55% Analysis Date = 02/06/15 Pct Recovery = 55% Analysis Date = 02/02/15 Pct Recovery = 55% Analysis Date = 02/02/15 Pct Recovery = 55% Analysis Date = 01/28/15 Pct Recovery = 55% Analysis Date = 01/28/15 Pct Recovery = 55% Analysis Date = 01/24/15 Pct Recovery = 56% Analysis Date = 01/24/15 Pct Recovery = 56% Analysis Date = 01/19/15 Pct Recovery = 56% Analysis Date = 01/19/15 Pct Recovery = 56% Analysis Date = 01/14/15 Pct Recovery = 56% Analysis Date = 01/14/15 Pct Recovery = 56% Analysis Date = 01/10/15 Pct Recovery = 57% Analysis Date = 01/10/15 Pct Recovery = 57% Analysis Date = 01/05/15 Pct Recovery = 57% Analysis Date = 01/05/15 Pct Recovery = 57% Analysis Date = 01/01/15 Pct Recovery = 57% Analysis Date = 01/01/15 Pct Recovery = 57% Analysis Date = 12/27/14 Pct Recovery = 57% Analysis Date = 12/27/14 Pct Recovery = 57% Analysis Date = 12/23/14 Pct Recovery = 58% Analysis Date = 12/23/14 Pct Recovery = 58% Analysis Date = 12/18/14 Pct Recovery = 58% Analysis Date = 12/18/14 Pct Recovery = 58% Analysis Date = 12/14/14 Pct Recovery = 58% Analysis Date = 12/14/14 Pct Recovery = 58% Analysis Date = 12/09/14 Pct Recovery = 59% Analysis Date = 12/09/14 Pct Recovery = 59% Analysis Date = 12/05/14 Pct Recovery = 59% Analysis Date = 12/05/14 Pct Recovery = 59% Analysis Date = 11/30/14 Pct Recovery = 59% Analysis Date = 11/30/14 Pct Recovery = 59% Analysis Date = 11/26/14 Pct Recovery = 59% Analysis Date = 11/26/14 Pct Recovery = 59% Analysis Date = 11/21/14 Pct Recovery = 60% Analysis Date = 11/21/14 Pct Recovery = 60% Analysis Date = 11/16/14 Pct Recovery = 60% Analysis Date = 11/16/14 Pct Recovery = 60% Analysis Date = 11/12/14 Pct Recovery = 60% Analysis Date = 11/12/14 Pct Recovery = 60% Analysis Date = 11/07/14 Pct Recovery = 60% Analysis Date = 11/07/14 Pct Recovery = 60% Analysis Date = 11/03/14 Pct Recovery = 61% Analysis Date = 11/03/14 Pct Recovery = 61% Analysis Date = 10/29/14 Pct Recovery = 61% Analysis Date = 10/29/14 Pct Recovery = 61% Analysis Date = 10/25/14 Pct Recovery = 61% Analysis Date = 10/25/14 Pct Recovery = 61% Analysis Date = 10/20/14 Pct Recovery = 62% Analysis Date = 10/20/14 Pct Recovery = 62% Analysis Date = 10/16/14 Pct Recovery = 62% Analysis Date = 10/16/14 Pct Recovery = 62% Analysis Date = 10/11/14 Pct Recovery = 62% Analysis Date = 10/11/14 Pct Recovery = 62% Analysis Date = 10/07/14 Pct Recovery = 62% Analysis Date = 10/07/14 Pct Recovery = 62% Analysis Date = 10/02/14 Pct Recovery = 63% Analysis Date = 10/02/14 Pct Recovery = 63% Analysis Date = 09/28/14 Pct Recovery = 63% Analysis Date = 09/28/14 Pct Recovery = 63% Analysis Date = 09/23/14 Pct Recovery = 63% Analysis Date = 09/23/14 Pct Recovery = 63% Analysis Date = 09/19/14 Pct Recovery = 63% Analysis Date = 09/19/14 Pct Recovery = 63% Analysis Date = 09/14/14 Pct Recovery = 64% Analysis Date = 09/14/14 Pct Recovery = 64% Analysis Date = 09/09/14 Pct Recovery = 64% Analysis Date = 09/09/14 Pct Recovery = 64% Analysis Date = 09/05/14 Pct Recovery = 64% Analysis Date = 09/05/14 Pct Recovery = 64% Analysis Date = 08/31/14 Pct Recovery = 65% Analysis Date = 08/31/14 Pct Recovery = 65% Analysis Date = 08/27/14 Pct Recovery = 65% Analysis Date = 08/27/14 Pct Recovery = 65% Analysis Date = 08/22/14 Pct Recovery = 65% Analysis Date = 08/22/14 Pct Recovery = 65% Analysis Date = 08/18/14 Pct Recovery = 65% Analysis Date = 08/18/14 Pct Recovery = 65% Analysis Date = 08/13/14 Pct Recovery = 66% Analysis Date = 08/13/14 Pct Recovery = 66% Analysis Date = 08/09/14 Pct Recovery = 66% Analysis Date = 08/09/14 Pct Recovery = 66% Analysis Date = 08/04/14 Pct Recovery = 66% Analysis Date = 08/04/14 Pct Recovery = 66% Analysis Date = 07/31/14 Pct Recovery = 66% Analysis Date = 07/31/14 Pct Recovery = 66% Analysis Date = 07/26/14 Pct Recovery = 67% Analysis Date = 07/26/14 Pct Recovery = 67% Analysis Date = 07/22/14 Pct Recovery = 67% Analysis Date = 07/22/14 Pct Recovery = 67% Analysis Date = 07/17/14 Pct Recovery = 67% Analysis Date = 07/17/14 Pct Recovery = 67% Analysis Date = 07/13/14 Pct Recovery = 68% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
CIMETIDINE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 1 68% . 68% 0%
>= Reporting Level 36 48% 25% 47% 27%
Total 37 48% 24% 49% 28%

Sample Statistics
CIMETIDINE

Characteristic N % % Basis
Plotted 37 48% Spiked
Estimated Values 37 48% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 6 8% Spiked
Spiked 77 .  
False Negatives 34 44% 34 out of 77
Not Spiked 38 .  
False Positives 0 0% 0 out of 38

BQS OBSP Determination:
CITALOPRAM
METHOD: 2440 , TESTIDCODE: 67505LCM56
Open Data Set

Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 49% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 50% Analysis Date = 01/17/16 SpikeMix = ERA 0406-15-09: 80 µl & ERA 0406-15-07A: 80 µl Pct Recovery = 68% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 80 µl & Abs 051315: 80 µl Pct Recovery = 130% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 80 µl & ERA 0406-15-08: 80 µl Pct Recovery = 51% Analysis Date = 11/04/15 SpikeMix = Abs 052215: 80 µl & Abs 050115: 80 µl Pct Recovery = 48% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 34% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 40% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 59% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 63% Analysis Date = 04/29/15 SpikeMix = ERA 0319-14-05: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 60% Analysis Date = 02/06/15 SpikeMix = Abs 041814: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 52% Analysis Date = 12/06/14 SpikeMix = ERA 0318-14-02: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 44% Analysis Date = 10/11/14 SpikeMix = ERA 0318-14-02: 60 µl & ERA 0319-14-04: 60 µl Pct Recovery = 49% Analysis Date = 08/21/14 SpikeMix = ERA 0318-14-02: 60 µl & Abs 041714: 60 µl Pct Recovery = 32% Analysis Date = 07/26/14 SpikeMix = ERA 0319-14-05: 60 µl & ERA 0318-14-02: 60 µl Pct Recovery = 61% Analysis Date = 12/07/14 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 45% Analysis Date = 10/25/14 SpikeMix = Abs 041614: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 45% Analysis Date = 06/22/14 SpikeMix = Abs 041814: 60 µl & Abs 041614: 60 µl Pct Recovery = 61% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-07A: 40 µl & Abs 051315: 40 µl Pct Recovery = 51% Analysis Date = 11/04/15 SpikeMix = ERA 0406-15-07A: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 59% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 100% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 85% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 36% Analysis Date = 02/23/16 SpikeMix = Abs 052215: 40 µl & Abs 050115: 40 µl Pct Recovery = 55% Analysis Date = 07/31/15 SpikeMix = ERA 0406-15-09: 40 µl & Abs 050115: 40 µl Pct Recovery = 58% Analysis Date = 07/30/15 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 62% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 43% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 46% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 50% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 45% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 26% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 40% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 32% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 36% Analysis Date = 12/07/14 SpikeMix = ERA 0318-14-02: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 54% Analysis Date = 11/04/14 SpikeMix = Abs 041814: 8 µl & ERA 0318-14-02: 8 µl Pct Recovery = 28% Analysis Date = 04/30/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 45% Analysis Date = 10/24/14 SpikeMix = ERA 0319-14-05: 8 µl & Abs 041614: 8 µl Pct Recovery = 40% Analysis Date = 10/10/14 SpikeMix = Abs 041814: 30 µl & ERA 0318-14-02: 30 µl Pct Recovery = 33% Analysis Date = 08/30/14 SpikeMix = ERA 0318-14-02: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 52% Analysis Date = 07/20/14 SpikeMix = ERA 0318-14-02: 30 µl & Abs 041714: 30 µl Pct Recovery = 37% Analysis Date = 09/12/14 SpikeMix = Abs 041614: 30 µl & ERA 0319-14-04: 30 µl Pct Recovery = 17% Analysis Date = 07/13/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 50% Analysis Date = 06/28/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 47% Analysis Date = 05/30/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 35% Analysis Date = 05/17/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 43% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 35% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 59% Analysis Date = 04/27/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 99% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 74% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 56% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 50% Analysis Date = 11/24/15 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 59% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-09: 20 µl Pct Recovery = 118% Analysis Date = 09/15/15 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 69% Analysis Date = 11/25/15 SpikeMix = Abs 050115: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 79% Analysis Date = 11/24/15 SpikeMix = ERA 0406-15-09: 20 µl & Abs 050115: 20 µl Pct Recovery = 71% Analysis Date = 08/27/15 SpikeMix = Abs 052215: 20 µl & Abs 050115: 20 µl Pct Recovery = 39% Analysis Date = 08/11/15 SpikeMix = Abs 050115: 20 µl & Abs 051315: 20 µl Pct Recovery = 21% Analysis Date = 07/09/15 SpikeMix = Abs 050115: 20 µl & Abs 052215: 20 µl Pct Recovery = 26% Analysis Date = 01/18/17 Pct Recovery = 38% Analysis Date = 01/14/17 Pct Recovery = 38% Analysis Date = 01/14/17 Pct Recovery = 38% Analysis Date = 01/09/17 Pct Recovery = 39% Analysis Date = 01/09/17 Pct Recovery = 39% Analysis Date = 01/04/17 Pct Recovery = 39% Analysis Date = 01/04/17 Pct Recovery = 39% Analysis Date = 12/30/16 Pct Recovery = 39% Analysis Date = 12/30/16 Pct Recovery = 39% Analysis Date = 12/25/16 Pct Recovery = 40% Analysis Date = 12/25/16 Pct Recovery = 40% Analysis Date = 12/20/16 Pct Recovery = 40% Analysis Date = 12/20/16 Pct Recovery = 40% Analysis Date = 12/15/16 Pct Recovery = 40% Analysis Date = 12/15/16 Pct Recovery = 40% Analysis Date = 12/10/16 Pct Recovery = 41% Analysis Date = 12/10/16 Pct Recovery = 41% Analysis Date = 12/05/16 Pct Recovery = 41% Analysis Date = 12/05/16 Pct Recovery = 41% Analysis Date = 12/01/16 Pct Recovery = 42% Analysis Date = 12/01/16 Pct Recovery = 42% Analysis Date = 11/26/16 Pct Recovery = 42% Analysis Date = 11/26/16 Pct Recovery = 42% Analysis Date = 11/21/16 Pct Recovery = 42% Analysis Date = 11/21/16 Pct Recovery = 42% Analysis Date = 11/16/16 Pct Recovery = 43% Analysis Date = 11/16/16 Pct Recovery = 43% Analysis Date = 11/11/16 Pct Recovery = 43% Analysis Date = 11/11/16 Pct Recovery = 43% Analysis Date = 11/06/16 Pct Recovery = 43% Analysis Date = 11/06/16 Pct Recovery = 43% Analysis Date = 11/01/16 Pct Recovery = 44% Analysis Date = 11/01/16 Pct Recovery = 44% Analysis Date = 10/27/16 Pct Recovery = 44% Analysis Date = 10/27/16 Pct Recovery = 44% Analysis Date = 10/22/16 Pct Recovery = 44% Analysis Date = 10/22/16 Pct Recovery = 44% Analysis Date = 10/18/16 Pct Recovery = 45% Analysis Date = 10/18/16 Pct Recovery = 45% Analysis Date = 10/13/16 Pct Recovery = 45% Analysis Date = 10/13/16 Pct Recovery = 45% Analysis Date = 10/08/16 Pct Recovery = 45% Analysis Date = 10/08/16 Pct Recovery = 45% Analysis Date = 10/03/16 Pct Recovery = 46% Analysis Date = 10/03/16 Pct Recovery = 46% Analysis Date = 09/28/16 Pct Recovery = 46% Analysis Date = 09/28/16 Pct Recovery = 46% Analysis Date = 09/23/16 Pct Recovery = 47% Analysis Date = 09/23/16 Pct Recovery = 47% Analysis Date = 09/18/16 Pct Recovery = 47% Analysis Date = 09/18/16 Pct Recovery = 47% Analysis Date = 09/13/16 Pct Recovery = 47% Analysis Date = 09/13/16 Pct Recovery = 47% Analysis Date = 09/08/16 Pct Recovery = 48% Analysis Date = 09/08/16 Pct Recovery = 48% Analysis Date = 09/04/16 Pct Recovery = 48% Analysis Date = 09/04/16 Pct Recovery = 48% Analysis Date = 08/30/16 Pct Recovery = 48% Analysis Date = 08/30/16 Pct Recovery = 48% Analysis Date = 08/25/16 Pct Recovery = 49% Analysis Date = 08/25/16 Pct Recovery = 49% Analysis Date = 08/20/16 Pct Recovery = 49% Analysis Date = 08/20/16 Pct Recovery = 49% Analysis Date = 08/15/16 Pct Recovery = 49% Analysis Date = 08/15/16 Pct Recovery = 49% Analysis Date = 08/10/16 Pct Recovery = 50% Analysis Date = 08/10/16 Pct Recovery = 50% Analysis Date = 08/05/16 Pct Recovery = 50% Analysis Date = 08/05/16 Pct Recovery = 50% Analysis Date = 07/31/16 Pct Recovery = 50% Analysis Date = 07/31/16 Pct Recovery = 50% Analysis Date = 07/26/16 Pct Recovery = 51% Analysis Date = 07/26/16 Pct Recovery = 51% Analysis Date = 07/22/16 Pct Recovery = 51% Analysis Date = 07/22/16 Pct Recovery = 51% Analysis Date = 07/17/16 Pct Recovery = 51% Analysis Date = 07/17/16 Pct Recovery = 51% Analysis Date = 07/12/16 Pct Recovery = 52% Analysis Date = 07/12/16 Pct Recovery = 52% Analysis Date = 07/07/16 Pct Recovery = 52% Analysis Date = 07/07/16 Pct Recovery = 52% Analysis Date = 07/02/16 Pct Recovery = 52% Analysis Date = 07/02/16 Pct Recovery = 52% Analysis Date = 06/27/16 Pct Recovery = 53% Analysis Date = 06/27/16 Pct Recovery = 53% Analysis Date = 06/22/16 Pct Recovery = 53% Analysis Date = 06/22/16 Pct Recovery = 53% Analysis Date = 06/17/16 Pct Recovery = 53% Analysis Date = 06/17/16 Pct Recovery = 53% Analysis Date = 06/12/16 Pct Recovery = 54% Analysis Date = 06/12/16 Pct Recovery = 54% Analysis Date = 06/08/16 Pct Recovery = 54% Analysis Date = 06/08/16 Pct Recovery = 54% Analysis Date = 06/03/16 Pct Recovery = 54% Analysis Date = 06/03/16 Pct Recovery = 54% Analysis Date = 05/29/16 Pct Recovery = 55% Analysis Date = 05/29/16 Pct Recovery = 55% Analysis Date = 05/24/16 Pct Recovery = 55% Analysis Date = 05/24/16 Pct Recovery = 55% Analysis Date = 05/19/16 Pct Recovery = 56% Analysis Date = 05/19/16 Pct Recovery = 56% Analysis Date = 05/14/16 Pct Recovery = 56% Analysis Date = 05/14/16 Pct Recovery = 56% Analysis Date = 05/09/16 Pct Recovery = 56% Analysis Date = 05/09/16 Pct Recovery = 56% Analysis Date = 05/04/16 Pct Recovery = 57% Analysis Date = 05/04/16 Pct Recovery = 57% Analysis Date = 04/29/16 Pct Recovery = 57% Analysis Date = 04/29/16 Pct Recovery = 57% Analysis Date = 04/25/16 Pct Recovery = 58% Analysis Date = 04/25/16 Pct Recovery = 58% Analysis Date = 04/20/16 Pct Recovery = 58% Analysis Date = 04/20/16 Pct Recovery = 58% Analysis Date = 04/15/16 Pct Recovery = 59% Analysis Date = 04/15/16 Pct Recovery = 59% Analysis Date = 04/10/16 Pct Recovery = 59% Analysis Date = 04/10/16 Pct Recovery = 59% Analysis Date = 04/05/16 Pct Recovery = 60% Analysis Date = 04/05/16 Pct Recovery = 60% Analysis Date = 03/31/16 Pct Recovery = 60% Analysis Date = 03/31/16 Pct Recovery = 60% Analysis Date = 03/26/16 Pct Recovery = 61% Analysis Date = 03/26/16 Pct Recovery = 61% Analysis Date = 03/21/16 Pct Recovery = 61% Analysis Date = 03/21/16 Pct Recovery = 61% Analysis Date = 03/16/16 Pct Recovery = 62% Analysis Date = 03/16/16 Pct Recovery = 62% Analysis Date = 03/12/16 Pct Recovery = 62% Analysis Date = 03/12/16 Pct Recovery = 62% Analysis Date = 03/07/16 Pct Recovery = 63% Analysis Date = 03/07/16 Pct Recovery = 63% Analysis Date = 03/02/16 Pct Recovery = 63% Analysis Date = 03/02/16 Pct Recovery = 63% Analysis Date = 02/26/16 Pct Recovery = 64% Analysis Date = 02/26/16 Pct Recovery = 64% Analysis Date = 02/21/16 Pct Recovery = 64% Analysis Date = 02/21/16 Pct Recovery = 64% Analysis Date = 02/16/16 Pct Recovery = 64% Analysis Date = 02/16/16 Pct Recovery = 64% Analysis Date = 02/11/16 Pct Recovery = 64% Analysis Date = 02/11/16 Pct Recovery = 64% Analysis Date = 02/06/16 Pct Recovery = 64% Analysis Date = 02/06/16 Pct Recovery = 64% Analysis Date = 02/01/16 Pct Recovery = 64% Analysis Date = 02/01/16 Pct Recovery = 64% Analysis Date = 01/28/16 Pct Recovery = 64% Analysis Date = 01/28/16 Pct Recovery = 64% Analysis Date = 01/23/16 Pct Recovery = 64% Analysis Date = 01/23/16 Pct Recovery = 64% Analysis Date = 01/18/16 Pct Recovery = 64% Analysis Date = 01/18/16 Pct Recovery = 64% Analysis Date = 01/13/16 Pct Recovery = 64% Analysis Date = 01/13/16 Pct Recovery = 64% Analysis Date = 01/08/16 Pct Recovery = 64% Analysis Date = 01/08/16 Pct Recovery = 64% Analysis Date = 01/03/16 Pct Recovery = 64% Analysis Date = 01/03/16 Pct Recovery = 64% Analysis Date = 12/29/15 Pct Recovery = 64% Analysis Date = 12/29/15 Pct Recovery = 64% Analysis Date = 12/24/15 Pct Recovery = 64% Analysis Date = 12/24/15 Pct Recovery = 64% Analysis Date = 12/19/15 Pct Recovery = 64% Analysis Date = 12/19/15 Pct Recovery = 64% Analysis Date = 12/15/15 Pct Recovery = 64% Analysis Date = 12/15/15 Pct Recovery = 64% Analysis Date = 12/10/15 Pct Recovery = 64% Analysis Date = 12/10/15 Pct Recovery = 64% Analysis Date = 12/05/15 Pct Recovery = 64% Analysis Date = 12/05/15 Pct Recovery = 64% Analysis Date = 11/30/15 Pct Recovery = 63% Analysis Date = 11/30/15 Pct Recovery = 63% Analysis Date = 11/25/15 Pct Recovery = 63% Analysis Date = 11/25/15 Pct Recovery = 63% Analysis Date = 11/20/15 Pct Recovery = 63% Analysis Date = 11/20/15 Pct Recovery = 63% Analysis Date = 11/15/15 Pct Recovery = 63% Analysis Date = 11/15/15 Pct Recovery = 63% Analysis Date = 11/10/15 Pct Recovery = 63% Analysis Date = 11/10/15 Pct Recovery = 63% Analysis Date = 11/05/15 Pct Recovery = 62% Analysis Date = 11/05/15 Pct Recovery = 62% Analysis Date = 11/01/15 Pct Recovery = 62% Analysis Date = 11/01/15 Pct Recovery = 62% Analysis Date = 10/27/15 Pct Recovery = 62% Analysis Date = 10/27/15 Pct Recovery = 62% Analysis Date = 10/22/15 Pct Recovery = 62% Analysis Date = 10/22/15 Pct Recovery = 62% Analysis Date = 10/17/15 Pct Recovery = 61% Analysis Date = 10/17/15 Pct Recovery = 61% Analysis Date = 10/12/15 Pct Recovery = 61% Analysis Date = 10/12/15 Pct Recovery = 61% Analysis Date = 10/07/15 Pct Recovery = 61% Analysis Date = 10/07/15 Pct Recovery = 61% Analysis Date = 10/02/15 Pct Recovery = 61% Analysis Date = 10/02/15 Pct Recovery = 61% Analysis Date = 09/27/15 Pct Recovery = 61% Analysis Date = 09/27/15 Pct Recovery = 61% Analysis Date = 09/22/15 Pct Recovery = 61% Analysis Date = 09/22/15 Pct Recovery = 61% Analysis Date = 09/17/15 Pct Recovery = 60% Analysis Date = 09/17/15 Pct Recovery = 60% Analysis Date = 09/13/15 Pct Recovery = 60% Analysis Date = 09/13/15 Pct Recovery = 60% Analysis Date = 09/08/15 Pct Recovery = 60% Analysis Date = 09/08/15 Pct Recovery = 60% Analysis Date = 09/03/15 Pct Recovery = 60% Analysis Date = 09/03/15 Pct Recovery = 60% Analysis Date = 08/29/15 Pct Recovery = 60% Analysis Date = 08/29/15 Pct Recovery = 60% Analysis Date = 08/24/15 Pct Recovery = 59% Analysis Date = 08/24/15 Pct Recovery = 59% Analysis Date = 08/19/15 Pct Recovery = 59% Analysis Date = 08/19/15 Pct Recovery = 59% Analysis Date = 08/14/15 Pct Recovery = 59% Analysis Date = 08/14/15 Pct Recovery = 59% Analysis Date = 08/09/15 Pct Recovery = 59% Analysis Date = 08/09/15 Pct Recovery = 59% Analysis Date = 08/04/15 Pct Recovery = 59% Analysis Date = 08/04/15 Pct Recovery = 59% Analysis Date = 07/31/15 Pct Recovery = 58% Analysis Date = 07/31/15 Pct Recovery = 58% Analysis Date = 07/26/15 Pct Recovery = 58% Analysis Date = 07/26/15 Pct Recovery = 58% Analysis Date = 07/21/15 Pct Recovery = 58% Analysis Date = 07/21/15 Pct Recovery = 58% Analysis Date = 07/16/15 Pct Recovery = 58% Analysis Date = 07/16/15 Pct Recovery = 58% Analysis Date = 07/11/15 Pct Recovery = 57% Analysis Date = 07/11/15 Pct Recovery = 57% Analysis Date = 07/06/15 Pct Recovery = 57% Analysis Date = 07/06/15 Pct Recovery = 57% Analysis Date = 07/01/15 Pct Recovery = 57% Analysis Date = 07/01/15 Pct Recovery = 57% Analysis Date = 06/26/15 Pct Recovery = 56% Analysis Date = 06/26/15 Pct Recovery = 56% Analysis Date = 06/21/15 Pct Recovery = 56% Analysis Date = 06/21/15 Pct Recovery = 56% Analysis Date = 06/17/15 Pct Recovery = 56% Analysis Date = 06/17/15 Pct Recovery = 56% Analysis Date = 06/12/15 Pct Recovery = 55% Analysis Date = 06/12/15 Pct Recovery = 55% Analysis Date = 06/07/15 Pct Recovery = 55% Analysis Date = 06/07/15 Pct Recovery = 55% Analysis Date = 06/02/15 Pct Recovery = 55% Analysis Date = 06/02/15 Pct Recovery = 55% Analysis Date = 05/28/15 Pct Recovery = 55% Analysis Date = 05/28/15 Pct Recovery = 55% Analysis Date = 05/23/15 Pct Recovery = 54% Analysis Date = 05/23/15 Pct Recovery = 54% Analysis Date = 05/18/15 Pct Recovery = 54% Analysis Date = 05/18/15 Pct Recovery = 54% Analysis Date = 05/13/15 Pct Recovery = 54% Analysis Date = 05/13/15 Pct Recovery = 54% Analysis Date = 05/08/15 Pct Recovery = 53% Analysis Date = 05/08/15 Pct Recovery = 53% Analysis Date = 05/04/15 Pct Recovery = 53% Analysis Date = 05/04/15 Pct Recovery = 53% Analysis Date = 04/29/15 Pct Recovery = 53% Analysis Date = 04/29/15 Pct Recovery = 53% Analysis Date = 04/24/15 Pct Recovery = 52% Analysis Date = 04/24/15 Pct Recovery = 52% Analysis Date = 04/19/15 Pct Recovery = 52% Analysis Date = 04/19/15 Pct Recovery = 52% Analysis Date = 04/14/15 Pct Recovery = 52% Analysis Date = 04/14/15 Pct Recovery = 52% Analysis Date = 04/09/15 Pct Recovery = 52% Analysis Date = 04/09/15 Pct Recovery = 52% Analysis Date = 04/04/15 Pct Recovery = 52% Analysis Date = 04/04/15 Pct Recovery = 52% Analysis Date = 03/30/15 Pct Recovery = 51% Analysis Date = 03/30/15 Pct Recovery = 51% Analysis Date = 03/25/15 Pct Recovery = 51% Analysis Date = 03/25/15 Pct Recovery = 51% Analysis Date = 03/21/15 Pct Recovery = 51% Analysis Date = 03/21/15 Pct Recovery = 51% Analysis Date = 03/16/15 Pct Recovery = 51% Analysis Date = 03/16/15 Pct Recovery = 51% Analysis Date = 03/11/15 Pct Recovery = 50% Analysis Date = 03/11/15 Pct Recovery = 50% Analysis Date = 03/06/15 Pct Recovery = 50% Analysis Date = 03/06/15 Pct Recovery = 50% Analysis Date = 03/01/15 Pct Recovery = 50% Analysis Date = 03/01/15 Pct Recovery = 50% Analysis Date = 02/24/15 Pct Recovery = 50% Analysis Date = 02/24/15 Pct Recovery = 50% Analysis Date = 02/19/15 Pct Recovery = 50% Analysis Date = 02/19/15 Pct Recovery = 50% Analysis Date = 02/14/15 Pct Recovery = 49% Analysis Date = 02/14/15 Pct Recovery = 49% Analysis Date = 02/09/15 Pct Recovery = 49% Analysis Date = 02/09/15 Pct Recovery = 49% Analysis Date = 02/05/15 Pct Recovery = 49% Analysis Date = 02/05/15 Pct Recovery = 49% Analysis Date = 01/31/15 Pct Recovery = 49% Analysis Date = 01/31/15 Pct Recovery = 49% Analysis Date = 01/26/15 Pct Recovery = 48% Analysis Date = 01/26/15 Pct Recovery = 48% Analysis Date = 01/21/15 Pct Recovery = 48% Analysis Date = 01/21/15 Pct Recovery = 48% Analysis Date = 01/16/15 Pct Recovery = 48% Analysis Date = 01/16/15 Pct Recovery = 48% Analysis Date = 01/11/15 Pct Recovery = 48% Analysis Date = 01/11/15 Pct Recovery = 48% Analysis Date = 01/06/15 Pct Recovery = 48% Analysis Date = 01/06/15 Pct Recovery = 48% Analysis Date = 01/01/15 Pct Recovery = 47% Analysis Date = 01/01/15 Pct Recovery = 47% Analysis Date = 12/27/14 Pct Recovery = 47% Analysis Date = 12/27/14 Pct Recovery = 47% Analysis Date = 12/23/14 Pct Recovery = 47% Analysis Date = 12/23/14 Pct Recovery = 47% Analysis Date = 12/18/14 Pct Recovery = 47% Analysis Date = 12/18/14 Pct Recovery = 47% Analysis Date = 12/13/14 Pct Recovery = 46% Analysis Date = 12/13/14 Pct Recovery = 46% Analysis Date = 12/08/14 Pct Recovery = 46% Analysis Date = 12/08/14 Pct Recovery = 46% Analysis Date = 12/03/14 Pct Recovery = 46% Analysis Date = 12/03/14 Pct Recovery = 46% Analysis Date = 11/28/14 Pct Recovery = 46% Analysis Date = 11/28/14 Pct Recovery = 46% Analysis Date = 11/23/14 Pct Recovery = 46% Analysis Date = 11/23/14 Pct Recovery = 46% Analysis Date = 11/18/14 Pct Recovery = 46% Analysis Date = 11/18/14 Pct Recovery = 46% Analysis Date = 11/13/14 Pct Recovery = 46% Analysis Date = 11/13/14 Pct Recovery = 46% Analysis Date = 11/09/14 Pct Recovery = 45% Analysis Date = 11/09/14 Pct Recovery = 45% Analysis Date = 11/04/14 Pct Recovery = 45% Analysis Date = 11/04/14 Pct Recovery = 45% Analysis Date = 10/30/14 Pct Recovery = 45% Analysis Date = 10/30/14 Pct Recovery = 45% Analysis Date = 10/25/14 Pct Recovery = 45% Analysis Date = 10/25/14 Pct Recovery = 45% Analysis Date = 10/20/14 Pct Recovery = 45% Analysis Date = 10/20/14 Pct Recovery = 45% Analysis Date = 10/15/14 Pct Recovery = 45% Analysis Date = 10/15/14 Pct Recovery = 45% Analysis Date = 10/10/14 Pct Recovery = 45% Analysis Date = 10/10/14 Pct Recovery = 45% Analysis Date = 10/05/14 Pct Recovery = 44% Analysis Date = 10/05/14 Pct Recovery = 44% Analysis Date = 09/30/14 Pct Recovery = 44% Analysis Date = 09/30/14 Pct Recovery = 44% Analysis Date = 09/26/14 Pct Recovery = 44% Analysis Date = 09/26/14 Pct Recovery = 44% Analysis Date = 09/21/14 Pct Recovery = 44% Analysis Date = 09/21/14 Pct Recovery = 44% Analysis Date = 09/16/14 Pct Recovery = 44% Analysis Date = 09/16/14 Pct Recovery = 44% Analysis Date = 09/11/14 Pct Recovery = 44% Analysis Date = 09/11/14 Pct Recovery = 44% Analysis Date = 09/06/14 Pct Recovery = 44% Analysis Date = 09/06/14 Pct Recovery = 44% Analysis Date = 09/01/14 Pct Recovery = 43% Analysis Date = 09/01/14 Pct Recovery = 43% Analysis Date = 08/27/14 Pct Recovery = 43% Analysis Date = 08/27/14 Pct Recovery = 43% Analysis Date = 08/22/14 Pct Recovery = 43% Analysis Date = 08/22/14 Pct Recovery = 43% Analysis Date = 08/17/14 Pct Recovery = 43% Analysis Date = 08/17/14 Pct Recovery = 43% Analysis Date = 08/13/14 Pct Recovery = 43% Analysis Date = 08/13/14 Pct Recovery = 43% Analysis Date = 08/08/14 Pct Recovery = 43% Analysis Date = 08/08/14 Pct Recovery = 43% Analysis Date = 08/03/14 Pct Recovery = 43% Analysis Date = 08/03/14 Pct Recovery = 43% Analysis Date = 07/29/14 Pct Recovery = 43% Analysis Date = 07/29/14 Pct Recovery = 43% Analysis Date = 07/24/14 Pct Recovery = 42% Analysis Date = 07/24/14 Pct Recovery = 42% Analysis Date = 07/19/14 Pct Recovery = 42% Analysis Date = 07/19/14 Pct Recovery = 42% Analysis Date = 07/14/14 Pct Recovery = 42% Analysis Date = 07/14/14 Pct Recovery = 42% Analysis Date = 07/09/14 Pct Recovery = 42% Analysis Date = 07/09/14 Pct Recovery = 42% Analysis Date = 07/04/14 Pct Recovery = 42% Analysis Date = 07/04/14 Pct Recovery = 42% Analysis Date = 06/30/14 Pct Recovery = 42% Analysis Date = 06/30/14 Pct Recovery = 42% Analysis Date = 06/25/14 Pct Recovery = 42% Analysis Date = 06/25/14 Pct Recovery = 42% Analysis Date = 06/20/14 Pct Recovery = 42% Analysis Date = 06/20/14 Pct Recovery = 42% Analysis Date = 06/15/14 Pct Recovery = 42% Analysis Date = 06/15/14 Pct Recovery = 42% Analysis Date = 06/10/14 Pct Recovery = 42% Analysis Date = 06/10/14 Pct Recovery = 42% Analysis Date = 06/05/14 Pct Recovery = 41% Analysis Date = 06/05/14 Pct Recovery = 41% Analysis Date = 05/31/14 Pct Recovery = 41% Analysis Date = 05/31/14 Pct Recovery = 41% Analysis Date = 05/26/14 Pct Recovery = 41% Analysis Date = 05/26/14 Pct Recovery = 41% Analysis Date = 05/21/14 Pct Recovery = 41% Analysis Date = 05/21/14 Pct Recovery = 41% Analysis Date = 05/17/14 Pct Recovery = 41% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
CITALOPRAM

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 61 52% 21% 50% 14%
Total 61 52% 21% 50% 14%

Sample Statistics
CITALOPRAM

Characteristic N % % Basis
Plotted 61 91% Spiked
Estimated Values 14 21% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 1 1% Spiked
Spiked 67 .  
False Negatives 5 7% 5 out of 67
Not Spiked 48 .  
False Positives 0 0% 0 out of 48

BQS OBSP Determination:
CLONIDINE
METHOD: 2440 , TESTIDCODE: 67518LCM56
Open Data Set

Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 82% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 80% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 80 µl & ERA 0406-15-08: 80 µl Pct Recovery = 83% Analysis Date = 11/05/15 SpikeMix = ERA 0406-15-08: 80 µl & Abs 052215: 80 µl Pct Recovery = 85% Analysis Date = 11/24/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 84% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 80 µl & Abs 051315: 80 µl Pct Recovery = 83% Analysis Date = 10/01/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 89% Analysis Date = 09/24/16 SpikeMix = Crescent EN160610015: 80 µl & Abs 061416: 80 µl Pct Recovery = 92% Analysis Date = 09/24/16 SpikeMix = Abs 061416: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 87% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 106% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 104% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 103% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 100% Analysis Date = 11/18/16 SpikeMix = ERA 04281604: 80 µl & ERA 04281603: 80 µl Pct Recovery = 81% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & ERA 04281604: 80 µl Pct Recovery = 80% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-04: 15 µl & Abs 041814: 15 µl Pct Recovery = 83% Analysis Date = 02/06/15 SpikeMix = Abs 041814: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 85% Analysis Date = 07/12/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 92% Analysis Date = 06/22/14 SpikeMix = Abs 041814: 60 µl & Abs 041614: 60 µl Pct Recovery = 114% Analysis Date = 05/21/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 89% Analysis Date = 05/07/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 102% Analysis Date = 04/29/15 SpikeMix = ERA 0319-14-05: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 94% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 86% Analysis Date = 01/16/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 85% Analysis Date = 12/07/14 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 75% Analysis Date = 12/06/14 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 69% Analysis Date = 08/28/14 SpikeMix = ERA 0319-14-04: 60 µl & ERA 0319-14-05: 60 µl Pct Recovery = 72% Analysis Date = 07/26/14 SpikeMix = ERA 0319-14-05: 60 µl & ERA 0318-14-02: 60 µl Pct Recovery = 98% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-08: 40 µl & Abs 052215: 40 µl Pct Recovery = 73% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 75% Analysis Date = 11/04/15 SpikeMix = ERA 0406-15-07A: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 75% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-08: 40 µl & ERA 0406-15-09: 40 µl Pct Recovery = 68% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 81% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 67% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-07A: 40 µl & Abs 051315: 40 µl Pct Recovery = 67% Analysis Date = 07/31/15 SpikeMix = Abs 051315: 40 µl & Abs 052215: 40 µl Pct Recovery = 77% Analysis Date = 07/30/15 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 88% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 80% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 78% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 78% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 81% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 67% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 65% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 65% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 70% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 101% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 120% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 91% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 93% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 84% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 80% Analysis Date = 04/10/15 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 78% Analysis Date = 11/04/14 SpikeMix = Abs 041814: 8 µl & ERA 0318-14-02: 8 µl Pct Recovery = 90% Analysis Date = 10/11/14 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 74% Analysis Date = 11/04/14 SpikeMix = Abs 041714: 8 µl & ERA 0319-14-05: 8 µl Pct Recovery = 84% Analysis Date = 10/24/14 SpikeMix = ERA 0319-14-05: 8 µl & Abs 041614: 8 µl Pct Recovery = 79% Analysis Date = 10/10/14 SpikeMix = Abs 041714: 30 µl & Abs 041814: 30 µl Pct Recovery = 84% Analysis Date = 10/10/14 SpikeMix = Abs 041814: 30 µl & ERA 0318-14-02: 30 µl Pct Recovery = 76% Analysis Date = 07/13/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 92% Analysis Date = 05/30/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 100% Analysis Date = 08/30/14 SpikeMix = ERA 0318-14-02: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 78% Analysis Date = 08/16/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 48% Analysis Date = 07/13/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 87% Analysis Date = 04/27/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 100% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 68% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-08: 20 µl & ERA 0406-15-09: 20 µl Pct Recovery = 60% Analysis Date = 11/25/15 SpikeMix = Abs 050115: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 78% Analysis Date = 09/15/15 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 75% Analysis Date = 09/09/15 SpikeMix = ERA 0406-15-08: 20 µl & Abs 052215: 20 µl Pct Recovery = 92% Analysis Date = 02/23/16 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 75% Analysis Date = 08/11/15 SpikeMix = Abs 050115: 20 µl & Abs 051315: 20 µl Pct Recovery = 61% Analysis Date = 06/26/15 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 81% Analysis Date = 06/09/15 SpikeMix = Abs 051315: 20 µl & Abs 050115: 20 µl Pct Recovery = 76% Analysis Date = 04/09/16 SpikeMix = Abs 051315: 10 µl & ERA 0406-15-09: 10 µl Pct Recovery = 63% Analysis Date = 04/09/16 SpikeMix = Abs 051315: 10 µl & ERA 0406-15-09: 10 µl Pct Recovery = 82% Analysis Date = 01/04/17 Pct Recovery = 90% Analysis Date = 12/31/16 Pct Recovery = 90% Analysis Date = 12/31/16 Pct Recovery = 90% Analysis Date = 12/26/16 Pct Recovery = 90% Analysis Date = 12/26/16 Pct Recovery = 90% Analysis Date = 12/21/16 Pct Recovery = 90% Analysis Date = 12/21/16 Pct Recovery = 90% Analysis Date = 12/16/16 Pct Recovery = 89% Analysis Date = 12/16/16 Pct Recovery = 89% Analysis Date = 12/11/16 Pct Recovery = 89% Analysis Date = 12/11/16 Pct Recovery = 89% Analysis Date = 12/07/16 Pct Recovery = 89% Analysis Date = 12/07/16 Pct Recovery = 89% Analysis Date = 12/02/16 Pct Recovery = 89% Analysis Date = 12/02/16 Pct Recovery = 89% Analysis Date = 11/27/16 Pct Recovery = 88% Analysis Date = 11/27/16 Pct Recovery = 88% Analysis Date = 11/22/16 Pct Recovery = 88% Analysis Date = 11/22/16 Pct Recovery = 88% Analysis Date = 11/17/16 Pct Recovery = 88% Analysis Date = 11/17/16 Pct Recovery = 88% Analysis Date = 11/13/16 Pct Recovery = 88% Analysis Date = 11/13/16 Pct Recovery = 88% Analysis Date = 11/08/16 Pct Recovery = 88% Analysis Date = 11/08/16 Pct Recovery = 88% Analysis Date = 11/03/16 Pct Recovery = 87% Analysis Date = 11/03/16 Pct Recovery = 87% Analysis Date = 10/29/16 Pct Recovery = 87% Analysis Date = 10/29/16 Pct Recovery = 87% Analysis Date = 10/24/16 Pct Recovery = 87% Analysis Date = 10/24/16 Pct Recovery = 87% Analysis Date = 10/20/16 Pct Recovery = 87% Analysis Date = 10/20/16 Pct Recovery = 87% Analysis Date = 10/15/16 Pct Recovery = 86% Analysis Date = 10/15/16 Pct Recovery = 86% Analysis Date = 10/10/16 Pct Recovery = 86% Analysis Date = 10/10/16 Pct Recovery = 86% Analysis Date = 10/05/16 Pct Recovery = 86% Analysis Date = 10/05/16 Pct Recovery = 86% Analysis Date = 09/30/16 Pct Recovery = 86% Analysis Date = 09/30/16 Pct Recovery = 86% Analysis Date = 09/26/16 Pct Recovery = 86% Analysis Date = 09/26/16 Pct Recovery = 86% Analysis Date = 09/21/16 Pct Recovery = 85% Analysis Date = 09/21/16 Pct Recovery = 85% Analysis Date = 09/16/16 Pct Recovery = 85% Analysis Date = 09/16/16 Pct Recovery = 85% Analysis Date = 09/11/16 Pct Recovery = 85% Analysis Date = 09/11/16 Pct Recovery = 85% Analysis Date = 09/06/16 Pct Recovery = 85% Analysis Date = 09/06/16 Pct Recovery = 85% Analysis Date = 09/02/16 Pct Recovery = 84% Analysis Date = 09/02/16 Pct Recovery = 84% Analysis Date = 08/28/16 Pct Recovery = 84% Analysis Date = 08/28/16 Pct Recovery = 84% Analysis Date = 08/23/16 Pct Recovery = 84% Analysis Date = 08/23/16 Pct Recovery = 84% Analysis Date = 08/18/16 Pct Recovery = 84% Analysis Date = 08/18/16 Pct Recovery = 84% Analysis Date = 08/13/16 Pct Recovery = 84% Analysis Date = 08/13/16 Pct Recovery = 84% Analysis Date = 08/09/16 Pct Recovery = 83% Analysis Date = 08/09/16 Pct Recovery = 83% Analysis Date = 08/04/16 Pct Recovery = 83% Analysis Date = 08/04/16 Pct Recovery = 83% Analysis Date = 07/30/16 Pct Recovery = 83% Analysis Date = 07/30/16 Pct Recovery = 83% Analysis Date = 07/25/16 Pct Recovery = 83% Analysis Date = 07/25/16 Pct Recovery = 83% Analysis Date = 07/20/16 Pct Recovery = 83% Analysis Date = 07/20/16 Pct Recovery = 83% Analysis Date = 07/16/16 Pct Recovery = 83% Analysis Date = 07/16/16 Pct Recovery = 83% Analysis Date = 07/11/16 Pct Recovery = 82% Analysis Date = 07/11/16 Pct Recovery = 82% Analysis Date = 07/06/16 Pct Recovery = 82% Analysis Date = 07/06/16 Pct Recovery = 82% Analysis Date = 07/01/16 Pct Recovery = 82% Analysis Date = 07/01/16 Pct Recovery = 82% Analysis Date = 06/26/16 Pct Recovery = 82% Analysis Date = 06/26/16 Pct Recovery = 82% Analysis Date = 06/22/16 Pct Recovery = 82% Analysis Date = 06/22/16 Pct Recovery = 82% Analysis Date = 06/17/16 Pct Recovery = 82% Analysis Date = 06/17/16 Pct Recovery = 82% Analysis Date = 06/12/16 Pct Recovery = 81% Analysis Date = 06/12/16 Pct Recovery = 81% Analysis Date = 06/07/16 Pct Recovery = 81% Analysis Date = 06/07/16 Pct Recovery = 81% Analysis Date = 06/02/16 Pct Recovery = 81% Analysis Date = 06/02/16 Pct Recovery = 81% Analysis Date = 05/29/16 Pct Recovery = 81% Analysis Date = 05/29/16 Pct Recovery = 81% Analysis Date = 05/24/16 Pct Recovery = 81% Analysis Date = 05/24/16 Pct Recovery = 81% Analysis Date = 05/19/16 Pct Recovery = 81% Analysis Date = 05/19/16 Pct Recovery = 81% Analysis Date = 05/14/16 Pct Recovery = 80% Analysis Date = 05/14/16 Pct Recovery = 80% Analysis Date = 05/09/16 Pct Recovery = 80% Analysis Date = 05/09/16 Pct Recovery = 80% Analysis Date = 05/05/16 Pct Recovery = 80% Analysis Date = 05/05/16 Pct Recovery = 80% Analysis Date = 04/30/16 Pct Recovery = 80% Analysis Date = 04/30/16 Pct Recovery = 80% Analysis Date = 04/25/16 Pct Recovery = 80% Analysis Date = 04/25/16 Pct Recovery = 80% Analysis Date = 04/20/16 Pct Recovery = 80% Analysis Date = 04/20/16 Pct Recovery = 80% Analysis Date = 04/15/16 Pct Recovery = 79% Analysis Date = 04/15/16 Pct Recovery = 79% Analysis Date = 04/11/16 Pct Recovery = 79% Analysis Date = 04/11/16 Pct Recovery = 79% Analysis Date = 04/06/16 Pct Recovery = 79% Analysis Date = 04/06/16 Pct Recovery = 79% Analysis Date = 04/01/16 Pct Recovery = 79% Analysis Date = 04/01/16 Pct Recovery = 79% Analysis Date = 03/27/16 Pct Recovery = 79% Analysis Date = 03/27/16 Pct Recovery = 79% Analysis Date = 03/22/16 Pct Recovery = 79% Analysis Date = 03/22/16 Pct Recovery = 79% Analysis Date = 03/18/16 Pct Recovery = 79% Analysis Date = 03/18/16 Pct Recovery = 79% Analysis Date = 03/13/16 Pct Recovery = 79% Analysis Date = 03/13/16 Pct Recovery = 79% Analysis Date = 03/08/16 Pct Recovery = 79% Analysis Date = 03/08/16 Pct Recovery = 79% Analysis Date = 03/03/16 Pct Recovery = 79% Analysis Date = 03/03/16 Pct Recovery = 79% Analysis Date = 02/27/16 Pct Recovery = 79% Analysis Date = 02/27/16 Pct Recovery = 79% Analysis Date = 02/23/16 Pct Recovery = 79% Analysis Date = 02/23/16 Pct Recovery = 79% Analysis Date = 02/18/16 Pct Recovery = 79% Analysis Date = 02/18/16 Pct Recovery = 79% Analysis Date = 02/13/16 Pct Recovery = 79% Analysis Date = 02/13/16 Pct Recovery = 79% Analysis Date = 02/08/16 Pct Recovery = 79% Analysis Date = 02/08/16 Pct Recovery = 79% Analysis Date = 02/03/16 Pct Recovery = 79% Analysis Date = 02/03/16 Pct Recovery = 79% Analysis Date = 01/30/16 Pct Recovery = 79% Analysis Date = 01/30/16 Pct Recovery = 79% Analysis Date = 01/25/16 Pct Recovery = 78% Analysis Date = 01/25/16 Pct Recovery = 78% Analysis Date = 01/20/16 Pct Recovery = 78% Analysis Date = 01/20/16 Pct Recovery = 78% Analysis Date = 01/15/16 Pct Recovery = 78% Analysis Date = 01/15/16 Pct Recovery = 78% Analysis Date = 01/10/16 Pct Recovery = 78% Analysis Date = 01/10/16 Pct Recovery = 78% Analysis Date = 01/06/16 Pct Recovery = 78% Analysis Date = 01/06/16 Pct Recovery = 78% Analysis Date = 01/01/16 Pct Recovery = 78% Analysis Date = 01/01/16 Pct Recovery = 78% Analysis Date = 12/27/15 Pct Recovery = 78% Analysis Date = 12/27/15 Pct Recovery = 78% Analysis Date = 12/22/15 Pct Recovery = 78% Analysis Date = 12/22/15 Pct Recovery = 78% Analysis Date = 12/17/15 Pct Recovery = 78% Analysis Date = 12/17/15 Pct Recovery = 78% Analysis Date = 12/13/15 Pct Recovery = 78% Analysis Date = 12/13/15 Pct Recovery = 78% Analysis Date = 12/08/15 Pct Recovery = 78% Analysis Date = 12/08/15 Pct Recovery = 78% Analysis Date = 12/03/15 Pct Recovery = 78% Analysis Date = 12/03/15 Pct Recovery = 78% Analysis Date = 11/28/15 Pct Recovery = 78% Analysis Date = 11/28/15 Pct Recovery = 78% Analysis Date = 11/23/15 Pct Recovery = 78% Analysis Date = 11/23/15 Pct Recovery = 78% Analysis Date = 11/19/15 Pct Recovery = 78% Analysis Date = 11/19/15 Pct Recovery = 78% Analysis Date = 11/14/15 Pct Recovery = 78% Analysis Date = 11/14/15 Pct Recovery = 78% Analysis Date = 11/09/15 Pct Recovery = 78% Analysis Date = 11/09/15 Pct Recovery = 78% Analysis Date = 11/04/15 Pct Recovery = 79% Analysis Date = 11/04/15 Pct Recovery = 79% Analysis Date = 10/30/15 Pct Recovery = 79% Analysis Date = 10/30/15 Pct Recovery = 79% Analysis Date = 10/26/15 Pct Recovery = 79% Analysis Date = 10/26/15 Pct Recovery = 79% Analysis Date = 10/21/15 Pct Recovery = 79% Analysis Date = 10/21/15 Pct Recovery = 79% Analysis Date = 10/16/15 Pct Recovery = 79% Analysis Date = 10/16/15 Pct Recovery = 79% Analysis Date = 10/11/15 Pct Recovery = 79% Analysis Date = 10/11/15 Pct Recovery = 79% Analysis Date = 10/06/15 Pct Recovery = 79% Analysis Date = 10/06/15 Pct Recovery = 79% Analysis Date = 10/02/15 Pct Recovery = 79% Analysis Date = 10/02/15 Pct Recovery = 79% Analysis Date = 09/27/15 Pct Recovery = 79% Analysis Date = 09/27/15 Pct Recovery = 79% Analysis Date = 09/22/15 Pct Recovery = 79% Analysis Date = 09/22/15 Pct Recovery = 79% Analysis Date = 09/17/15 Pct Recovery = 79% Analysis Date = 09/17/15 Pct Recovery = 79% Analysis Date = 09/12/15 Pct Recovery = 79% Analysis Date = 09/12/15 Pct Recovery = 79% Analysis Date = 09/08/15 Pct Recovery = 79% Analysis Date = 09/08/15 Pct Recovery = 79% Analysis Date = 09/03/15 Pct Recovery = 80% Analysis Date = 09/03/15 Pct Recovery = 80% Analysis Date = 08/29/15 Pct Recovery = 80% Analysis Date = 08/29/15 Pct Recovery = 80% Analysis Date = 08/24/15 Pct Recovery = 80% Analysis Date = 08/24/15 Pct Recovery = 80% Analysis Date = 08/19/15 Pct Recovery = 80% Analysis Date = 08/19/15 Pct Recovery = 80% Analysis Date = 08/15/15 Pct Recovery = 80% Analysis Date = 08/15/15 Pct Recovery = 80% Analysis Date = 08/10/15 Pct Recovery = 80% Analysis Date = 08/10/15 Pct Recovery = 80% Analysis Date = 08/05/15 Pct Recovery = 80% Analysis Date = 08/05/15 Pct Recovery = 80% Analysis Date = 07/31/15 Pct Recovery = 80% Analysis Date = 07/31/15 Pct Recovery = 80% Analysis Date = 07/26/15 Pct Recovery = 80% Analysis Date = 07/26/15 Pct Recovery = 80% Analysis Date = 07/22/15 Pct Recovery = 80% Analysis Date = 07/22/15 Pct Recovery = 80% Analysis Date = 07/17/15 Pct Recovery = 80% Analysis Date = 07/17/15 Pct Recovery = 80% Analysis Date = 07/12/15 Pct Recovery = 80% Analysis Date = 07/12/15 Pct Recovery = 80% Analysis Date = 07/07/15 Pct Recovery = 80% Analysis Date = 07/07/15 Pct Recovery = 80% Analysis Date = 07/02/15 Pct Recovery = 80% Analysis Date = 07/02/15 Pct Recovery = 80% Analysis Date = 06/28/15 Pct Recovery = 80% Analysis Date = 06/28/15 Pct Recovery = 80% Analysis Date = 06/23/15 Pct Recovery = 80% Analysis Date = 06/23/15 Pct Recovery = 80% Analysis Date = 06/18/15 Pct Recovery = 80% Analysis Date = 06/18/15 Pct Recovery = 80% Analysis Date = 06/13/15 Pct Recovery = 80% Analysis Date = 06/13/15 Pct Recovery = 80% Analysis Date = 06/08/15 Pct Recovery = 81% Analysis Date = 06/08/15 Pct Recovery = 81% Analysis Date = 06/04/15 Pct Recovery = 81% Analysis Date = 06/04/15 Pct Recovery = 81% Analysis Date = 05/30/15 Pct Recovery = 81% Analysis Date = 05/30/15 Pct Recovery = 81% Analysis Date = 05/25/15 Pct Recovery = 81% Analysis Date = 05/25/15 Pct Recovery = 81% Analysis Date = 05/20/15 Pct Recovery = 81% Analysis Date = 05/20/15 Pct Recovery = 81% Analysis Date = 05/15/15 Pct Recovery = 81% Analysis Date = 05/15/15 Pct Recovery = 81% Analysis Date = 05/11/15 Pct Recovery = 81% Analysis Date = 05/11/15 Pct Recovery = 81% Analysis Date = 05/06/15 Pct Recovery = 81% Analysis Date = 05/06/15 Pct Recovery = 81% Analysis Date = 05/01/15 Pct Recovery = 81% Analysis Date = 05/01/15 Pct Recovery = 81% Analysis Date = 04/26/15 Pct Recovery = 81% Analysis Date = 04/26/15 Pct Recovery = 81% Analysis Date = 04/21/15 Pct Recovery = 81% Analysis Date = 04/21/15 Pct Recovery = 81% Analysis Date = 04/17/15 Pct Recovery = 81% Analysis Date = 04/17/15 Pct Recovery = 81% Analysis Date = 04/12/15 Pct Recovery = 81% Analysis Date = 04/12/15 Pct Recovery = 81% Analysis Date = 04/07/15 Pct Recovery = 81% Analysis Date = 04/07/15 Pct Recovery = 81% Analysis Date = 04/02/15 Pct Recovery = 81% Analysis Date = 04/02/15 Pct Recovery = 81% Analysis Date = 03/28/15 Pct Recovery = 81% Analysis Date = 03/28/15 Pct Recovery = 81% Analysis Date = 03/24/15 Pct Recovery = 81% Analysis Date = 03/24/15 Pct Recovery = 81% Analysis Date = 03/19/15 Pct Recovery = 81% Analysis Date = 03/19/15 Pct Recovery = 81% Analysis Date = 03/14/15 Pct Recovery = 82% Analysis Date = 03/14/15 Pct Recovery = 82% Analysis Date = 03/09/15 Pct Recovery = 82% Analysis Date = 03/09/15 Pct Recovery = 82% Analysis Date = 03/04/15 Pct Recovery = 82% Analysis Date = 03/04/15 Pct Recovery = 82% Analysis Date = 02/28/15 Pct Recovery = 82% Analysis Date = 02/28/15 Pct Recovery = 82% Analysis Date = 02/23/15 Pct Recovery = 82% Analysis Date = 02/23/15 Pct Recovery = 82% Analysis Date = 02/18/15 Pct Recovery = 82% Analysis Date = 02/18/15 Pct Recovery = 82% Analysis Date = 02/13/15 Pct Recovery = 82% Analysis Date = 02/13/15 Pct Recovery = 82% Analysis Date = 02/08/15 Pct Recovery = 82% Analysis Date = 02/08/15 Pct Recovery = 82% Analysis Date = 02/04/15 Pct Recovery = 82% Analysis Date = 02/04/15 Pct Recovery = 82% Analysis Date = 01/30/15 Pct Recovery = 82% Analysis Date = 01/30/15 Pct Recovery = 82% Analysis Date = 01/25/15 Pct Recovery = 82% Analysis Date = 01/25/15 Pct Recovery = 82% Analysis Date = 01/20/15 Pct Recovery = 82% Analysis Date = 01/20/15 Pct Recovery = 82% Analysis Date = 01/15/15 Pct Recovery = 82% Analysis Date = 01/15/15 Pct Recovery = 82% Analysis Date = 01/11/15 Pct Recovery = 82% Analysis Date = 01/11/15 Pct Recovery = 82% Analysis Date = 01/06/15 Pct Recovery = 83% Analysis Date = 01/06/15 Pct Recovery = 83% Analysis Date = 01/01/15 Pct Recovery = 83% Analysis Date = 01/01/15 Pct Recovery = 83% Analysis Date = 12/27/14 Pct Recovery = 83% Analysis Date = 12/27/14 Pct Recovery = 83% Analysis Date = 12/22/14 Pct Recovery = 83% Analysis Date = 12/22/14 Pct Recovery = 83% Analysis Date = 12/18/14 Pct Recovery = 83% Analysis Date = 12/18/14 Pct Recovery = 83% Analysis Date = 12/13/14 Pct Recovery = 83% Analysis Date = 12/13/14 Pct Recovery = 83% Analysis Date = 12/08/14 Pct Recovery = 83% Analysis Date = 12/08/14 Pct Recovery = 83% Analysis Date = 12/03/14 Pct Recovery = 83% Analysis Date = 12/03/14 Pct Recovery = 83% Analysis Date = 11/28/14 Pct Recovery = 83% Analysis Date = 11/28/14 Pct Recovery = 83% Analysis Date = 11/24/14 Pct Recovery = 83% Analysis Date = 11/24/14 Pct Recovery = 83% Analysis Date = 11/19/14 Pct Recovery = 83% Analysis Date = 11/19/14 Pct Recovery = 83% Analysis Date = 11/14/14 Pct Recovery = 84% Analysis Date = 11/14/14 Pct Recovery = 84% Analysis Date = 11/09/14 Pct Recovery = 84% Analysis Date = 11/09/14 Pct Recovery = 84% Analysis Date = 11/04/14 Pct Recovery = 84% Analysis Date = 11/04/14 Pct Recovery = 84% Analysis Date = 10/31/14 Pct Recovery = 84% Analysis Date = 10/31/14 Pct Recovery = 84% Analysis Date = 10/26/14 Pct Recovery = 84% Analysis Date = 10/26/14 Pct Recovery = 84% Analysis Date = 10/21/14 Pct Recovery = 84% Analysis Date = 10/21/14 Pct Recovery = 84% Analysis Date = 10/16/14 Pct Recovery = 84% Analysis Date = 10/16/14 Pct Recovery = 84% Analysis Date = 10/11/14 Pct Recovery = 84% Analysis Date = 10/11/14 Pct Recovery = 84% Analysis Date = 10/07/14 Pct Recovery = 84% Analysis Date = 10/07/14 Pct Recovery = 84% Analysis Date = 10/02/14 Pct Recovery = 84% Analysis Date = 10/02/14 Pct Recovery = 84% Analysis Date = 09/27/14 Pct Recovery = 84% Analysis Date = 09/27/14 Pct Recovery = 84% Analysis Date = 09/22/14 Pct Recovery = 85% Analysis Date = 09/22/14 Pct Recovery = 85% Analysis Date = 09/17/14 Pct Recovery = 85% Analysis Date = 09/17/14 Pct Recovery = 85% Analysis Date = 09/13/14 Pct Recovery = 85% Analysis Date = 09/13/14 Pct Recovery = 85% Analysis Date = 09/08/14 Pct Recovery = 85% Analysis Date = 09/08/14 Pct Recovery = 85% Analysis Date = 09/03/14 Pct Recovery = 85% Analysis Date = 09/03/14 Pct Recovery = 85% Analysis Date = 08/29/14 Pct Recovery = 85% Analysis Date = 08/29/14 Pct Recovery = 85% Analysis Date = 08/24/14 Pct Recovery = 85% Analysis Date = 08/24/14 Pct Recovery = 85% Analysis Date = 08/20/14 Pct Recovery = 85% Analysis Date = 08/20/14 Pct Recovery = 85% Analysis Date = 08/15/14 Pct Recovery = 85% Analysis Date = 08/15/14 Pct Recovery = 85% Analysis Date = 08/10/14 Pct Recovery = 85% Analysis Date = 08/10/14 Pct Recovery = 85% Analysis Date = 08/05/14 Pct Recovery = 85% Analysis Date = 08/05/14 Pct Recovery = 85% Analysis Date = 07/31/14 Pct Recovery = 86% Analysis Date = 07/31/14 Pct Recovery = 86% Analysis Date = 07/27/14 Pct Recovery = 86% Analysis Date = 07/27/14 Pct Recovery = 86% Analysis Date = 07/22/14 Pct Recovery = 86% Analysis Date = 07/22/14 Pct Recovery = 86% Analysis Date = 07/17/14 Pct Recovery = 86% Analysis Date = 07/17/14 Pct Recovery = 86% Analysis Date = 07/12/14 Pct Recovery = 86% Analysis Date = 07/12/14 Pct Recovery = 86% Analysis Date = 07/07/14 Pct Recovery = 86% Analysis Date = 07/07/14 Pct Recovery = 86% Analysis Date = 07/03/14 Pct Recovery = 86% Analysis Date = 07/03/14 Pct Recovery = 86% Analysis Date = 06/28/14 Pct Recovery = 86% Analysis Date = 06/28/14 Pct Recovery = 86% Analysis Date = 06/23/14 Pct Recovery = 86% Analysis Date = 06/23/14 Pct Recovery = 86% Analysis Date = 06/18/14 Pct Recovery = 86% Analysis Date = 06/18/14 Pct Recovery = 86% Analysis Date = 06/13/14 Pct Recovery = 86% Analysis Date = 06/13/14 Pct Recovery = 86% Analysis Date = 06/09/14 Pct Recovery = 87% Analysis Date = 06/09/14 Pct Recovery = 87% Analysis Date = 06/04/14 Pct Recovery = 87% Analysis Date = 06/04/14 Pct Recovery = 87% Analysis Date = 05/30/14 Pct Recovery = 87% Analysis Date = 05/30/14 Pct Recovery = 87% Analysis Date = 05/25/14 Pct Recovery = 87% Analysis Date = 05/25/14 Pct Recovery = 87% Analysis Date = 05/21/14 Pct Recovery = 87% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
CLONIDINE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 2 73% 14% 73% 14%
>= Reporting Level 73 83% 13% 81% 11%
Total 75 82% 13% 81% 11%

Sample Statistics
CLONIDINE

Characteristic N % % Basis
Plotted 75 100% Spiked
Estimated Values 21 28% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 75 .  
False Negatives 0 0% 0 out of 75
Not Spiked 40 .  
False Positives 0 0% 0 out of 40

BQS OBSP Determination:
CODEINE
METHOD: 2440 , TESTIDCODE: 67443LCM56
Open Data Set

Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 110% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 120% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 80 µl & ERA 0406-15-08: 80 µl Pct Recovery = 74% Analysis Date = 11/04/15 SpikeMix = Abs 052215: 80 µl & Abs 050115: 80 µl Pct Recovery = 80% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 87% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 85% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 80% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 86% Analysis Date = 11/18/16 SpikeMix = ERA 04281604: 80 µl & ERA 04281603: 80 µl Pct Recovery = 84% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & ERA 04281604: 80 µl Pct Recovery = 87% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 77% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 76% Analysis Date = 05/07/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 90% Analysis Date = 03/11/15 SpikeMix = ERA 0318-14-02: 15 µl & Abs 041714: 15 µl Pct Recovery = 104% Analysis Date = 01/16/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 72% Analysis Date = 12/06/14 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 75% Analysis Date = 08/21/14 SpikeMix = ERA 0318-14-02: 60 µl & Abs 041714: 60 µl Pct Recovery = 52% Analysis Date = 07/12/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 71% Analysis Date = 06/11/14 SpikeMix = Abs 041614: 60 µl & Abs 041714: 60 µl Pct Recovery = 78% Analysis Date = 05/21/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 83% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 70% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 63% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 53% Analysis Date = 02/23/16 SpikeMix = Abs 052215: 40 µl & Abs 050115: 40 µl Pct Recovery = 60% Analysis Date = 07/31/15 SpikeMix = ERA 0406-15-09: 40 µl & Abs 050115: 40 µl Pct Recovery = 88% Analysis Date = 07/30/15 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 91% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 129% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 135% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 93% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 90% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 81% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 86% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 87% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 91% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 67% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 86% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 77% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 100% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 104% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 98% Analysis Date = 11/04/14 SpikeMix = Abs 041714: 8 µl & ERA 0319-14-05: 8 µl Pct Recovery = 66% Analysis Date = 10/10/14 SpikeMix = Abs 041714: 30 µl & Abs 041814: 30 µl Pct Recovery = 95% Analysis Date = 07/20/14 SpikeMix = ERA 0318-14-02: 30 µl & Abs 041714: 30 µl Pct Recovery = 53% Analysis Date = 06/28/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 69% Analysis Date = 05/17/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 82% Analysis Date = 11/25/15 SpikeMix = Abs 050115: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 60% Analysis Date = 11/24/15 SpikeMix = ERA 0406-15-09: 20 µl & Abs 050115: 20 µl Pct Recovery = 65% Analysis Date = 08/27/15 SpikeMix = Abs 052215: 20 µl & Abs 050115: 20 µl Pct Recovery = 65% Analysis Date = 08/11/15 SpikeMix = Abs 050115: 20 µl & Abs 051315: 20 µl Pct Recovery = 60% Analysis Date = 07/09/15 SpikeMix = Abs 050115: 20 µl & Abs 052215: 20 µl Pct Recovery = 69% Analysis Date = 06/09/15 SpikeMix = Abs 051315: 20 µl & Abs 050115: 20 µl Pct Recovery = 65% Analysis Date = 01/18/17 Pct Recovery = 109% Analysis Date = 01/14/17 Pct Recovery = 108% Analysis Date = 01/14/17 Pct Recovery = 108% Analysis Date = 01/09/17 Pct Recovery = 108% Analysis Date = 01/09/17 Pct Recovery = 108% Analysis Date = 01/04/17 Pct Recovery = 107% Analysis Date = 01/04/17 Pct Recovery = 107% Analysis Date = 12/30/16 Pct Recovery = 106% Analysis Date = 12/30/16 Pct Recovery = 106% Analysis Date = 12/25/16 Pct Recovery = 105% Analysis Date = 12/25/16 Pct Recovery = 105% Analysis Date = 12/20/16 Pct Recovery = 104% Analysis Date = 12/20/16 Pct Recovery = 104% Analysis Date = 12/15/16 Pct Recovery = 103% Analysis Date = 12/15/16 Pct Recovery = 103% Analysis Date = 12/10/16 Pct Recovery = 102% Analysis Date = 12/10/16 Pct Recovery = 102% Analysis Date = 12/05/16 Pct Recovery = 102% Analysis Date = 12/05/16 Pct Recovery = 102% Analysis Date = 12/01/16 Pct Recovery = 101% Analysis Date = 12/01/16 Pct Recovery = 101% Analysis Date = 11/26/16 Pct Recovery = 100% Analysis Date = 11/26/16 Pct Recovery = 100% Analysis Date = 11/21/16 Pct Recovery = 99% Analysis Date = 11/21/16 Pct Recovery = 99% Analysis Date = 11/16/16 Pct Recovery = 98% Analysis Date = 11/16/16 Pct Recovery = 98% Analysis Date = 11/11/16 Pct Recovery = 97% Analysis Date = 11/11/16 Pct Recovery = 97% Analysis Date = 11/06/16 Pct Recovery = 97% Analysis Date = 11/06/16 Pct Recovery = 97% Analysis Date = 11/01/16 Pct Recovery = 96% Analysis Date = 11/01/16 Pct Recovery = 96% Analysis Date = 10/27/16 Pct Recovery = 95% Analysis Date = 10/27/16 Pct Recovery = 95% Analysis Date = 10/22/16 Pct Recovery = 94% Analysis Date = 10/22/16 Pct Recovery = 94% Analysis Date = 10/18/16 Pct Recovery = 93% Analysis Date = 10/18/16 Pct Recovery = 93% Analysis Date = 10/13/16 Pct Recovery = 92% Analysis Date = 10/13/16 Pct Recovery = 92% Analysis Date = 10/08/16 Pct Recovery = 92% Analysis Date = 10/08/16 Pct Recovery = 92% Analysis Date = 10/03/16 Pct Recovery = 91% Analysis Date = 10/03/16 Pct Recovery = 91% Analysis Date = 09/28/16 Pct Recovery = 90% Analysis Date = 09/28/16 Pct Recovery = 90% Analysis Date = 09/23/16 Pct Recovery = 89% Analysis Date = 09/23/16 Pct Recovery = 89% Analysis Date = 09/18/16 Pct Recovery = 88% Analysis Date = 09/18/16 Pct Recovery = 88% Analysis Date = 09/13/16 Pct Recovery = 88% Analysis Date = 09/13/16 Pct Recovery = 88% Analysis Date = 09/08/16 Pct Recovery = 87% Analysis Date = 09/08/16 Pct Recovery = 87% Analysis Date = 09/04/16 Pct Recovery = 86% Analysis Date = 09/04/16 Pct Recovery = 86% Analysis Date = 08/30/16 Pct Recovery = 85% Analysis Date = 08/30/16 Pct Recovery = 85% Analysis Date = 08/25/16 Pct Recovery = 85% Analysis Date = 08/25/16 Pct Recovery = 85% Analysis Date = 08/20/16 Pct Recovery = 84% Analysis Date = 08/20/16 Pct Recovery = 84% Analysis Date = 08/15/16 Pct Recovery = 83% Analysis Date = 08/15/16 Pct Recovery = 83% Analysis Date = 08/10/16 Pct Recovery = 82% Analysis Date = 08/10/16 Pct Recovery = 82% Analysis Date = 08/05/16 Pct Recovery = 82% Analysis Date = 08/05/16 Pct Recovery = 82% Analysis Date = 07/31/16 Pct Recovery = 81% Analysis Date = 07/31/16 Pct Recovery = 81% Analysis Date = 07/26/16 Pct Recovery = 81% Analysis Date = 07/26/16 Pct Recovery = 81% Analysis Date = 07/22/16 Pct Recovery = 81% Analysis Date = 07/22/16 Pct Recovery = 81% Analysis Date = 07/17/16 Pct Recovery = 80% Analysis Date = 07/17/16 Pct Recovery = 80% Analysis Date = 07/12/16 Pct Recovery = 80% Analysis Date = 07/12/16 Pct Recovery = 80% Analysis Date = 07/07/16 Pct Recovery = 79% Analysis Date = 07/07/16 Pct Recovery = 79% Analysis Date = 07/02/16 Pct Recovery = 79% Analysis Date = 07/02/16 Pct Recovery = 79% Analysis Date = 06/27/16 Pct Recovery = 78% Analysis Date = 06/27/16 Pct Recovery = 78% Analysis Date = 06/22/16 Pct Recovery = 78% Analysis Date = 06/22/16 Pct Recovery = 78% Analysis Date = 06/17/16 Pct Recovery = 77% Analysis Date = 06/17/16 Pct Recovery = 77% Analysis Date = 06/12/16 Pct Recovery = 77% Analysis Date = 06/12/16 Pct Recovery = 77% Analysis Date = 06/08/16 Pct Recovery = 76% Analysis Date = 06/08/16 Pct Recovery = 76% Analysis Date = 06/03/16 Pct Recovery = 76% Analysis Date = 06/03/16 Pct Recovery = 76% Analysis Date = 05/29/16 Pct Recovery = 75% Analysis Date = 05/29/16 Pct Recovery = 75% Analysis Date = 05/24/16 Pct Recovery = 75% Analysis Date = 05/24/16 Pct Recovery = 75% Analysis Date = 05/19/16 Pct Recovery = 75% Analysis Date = 05/19/16 Pct Recovery = 75% Analysis Date = 05/14/16 Pct Recovery = 74% Analysis Date = 05/14/16 Pct Recovery = 74% Analysis Date = 05/09/16 Pct Recovery = 74% Analysis Date = 05/09/16 Pct Recovery = 74% Analysis Date = 05/04/16 Pct Recovery = 73% Analysis Date = 05/04/16 Pct Recovery = 73% Analysis Date = 04/29/16 Pct Recovery = 73% Analysis Date = 04/29/16 Pct Recovery = 73% Analysis Date = 04/25/16 Pct Recovery = 72% Analysis Date = 04/25/16 Pct Recovery = 72% Analysis Date = 04/20/16 Pct Recovery = 72% Analysis Date = 04/20/16 Pct Recovery = 72% Analysis Date = 04/15/16 Pct Recovery = 72% Analysis Date = 04/15/16 Pct Recovery = 72% Analysis Date = 04/10/16 Pct Recovery = 72% Analysis Date = 04/10/16 Pct Recovery = 72% Analysis Date = 04/05/16 Pct Recovery = 72% Analysis Date = 04/05/16 Pct Recovery = 72% Analysis Date = 03/31/16 Pct Recovery = 72% Analysis Date = 03/31/16 Pct Recovery = 72% Analysis Date = 03/26/16 Pct Recovery = 72% Analysis Date = 03/26/16 Pct Recovery = 72% Analysis Date = 03/21/16 Pct Recovery = 72% Analysis Date = 03/21/16 Pct Recovery = 72% Analysis Date = 03/16/16 Pct Recovery = 72% Analysis Date = 03/16/16 Pct Recovery = 72% Analysis Date = 03/12/16 Pct Recovery = 72% Analysis Date = 03/12/16 Pct Recovery = 72% Analysis Date = 03/07/16 Pct Recovery = 72% Analysis Date = 03/07/16 Pct Recovery = 72% Analysis Date = 03/02/16 Pct Recovery = 72% Analysis Date = 03/02/16 Pct Recovery = 72% Analysis Date = 02/26/16 Pct Recovery = 72% Analysis Date = 02/26/16 Pct Recovery = 72% Analysis Date = 02/21/16 Pct Recovery = 72% Analysis Date = 02/21/16 Pct Recovery = 72% Analysis Date = 02/16/16 Pct Recovery = 72% Analysis Date = 02/16/16 Pct Recovery = 72% Analysis Date = 02/11/16 Pct Recovery = 72% Analysis Date = 02/11/16 Pct Recovery = 72% Analysis Date = 02/06/16 Pct Recovery = 72% Analysis Date = 02/06/16 Pct Recovery = 72% Analysis Date = 02/01/16 Pct Recovery = 72% Analysis Date = 02/01/16 Pct Recovery = 72% Analysis Date = 01/28/16 Pct Recovery = 72% Analysis Date = 01/28/16 Pct Recovery = 72% Analysis Date = 01/23/16 Pct Recovery = 72% Analysis Date = 01/23/16 Pct Recovery = 72% Analysis Date = 01/18/16 Pct Recovery = 72% Analysis Date = 01/18/16 Pct Recovery = 72% Analysis Date = 01/13/16 Pct Recovery = 71% Analysis Date = 01/13/16 Pct Recovery = 71% Analysis Date = 01/08/16 Pct Recovery = 71% Analysis Date = 01/08/16 Pct Recovery = 71% Analysis Date = 01/03/16 Pct Recovery = 71% Analysis Date = 01/03/16 Pct Recovery = 71% Analysis Date = 12/29/15 Pct Recovery = 71% Analysis Date = 12/29/15 Pct Recovery = 71% Analysis Date = 12/24/15 Pct Recovery = 71% Analysis Date = 12/24/15 Pct Recovery = 71% Analysis Date = 12/19/15 Pct Recovery = 71% Analysis Date = 12/19/15 Pct Recovery = 71% Analysis Date = 12/15/15 Pct Recovery = 71% Analysis Date = 12/15/15 Pct Recovery = 71% Analysis Date = 12/10/15 Pct Recovery = 71% Analysis Date = 12/10/15 Pct Recovery = 71% Analysis Date = 12/05/15 Pct Recovery = 71% Analysis Date = 12/05/15 Pct Recovery = 71% Analysis Date = 11/30/15 Pct Recovery = 71% Analysis Date = 11/30/15 Pct Recovery = 71% Analysis Date = 11/25/15 Pct Recovery = 71% Analysis Date = 11/25/15 Pct Recovery = 71% Analysis Date = 11/20/15 Pct Recovery = 71% Analysis Date = 11/20/15 Pct Recovery = 71% Analysis Date = 11/15/15 Pct Recovery = 71% Analysis Date = 11/15/15 Pct Recovery = 71% Analysis Date = 11/10/15 Pct Recovery = 71% Analysis Date = 11/10/15 Pct Recovery = 71% Analysis Date = 11/05/15 Pct Recovery = 71% Analysis Date = 11/05/15 Pct Recovery = 71% Analysis Date = 11/01/15 Pct Recovery = 71% Analysis Date = 11/01/15 Pct Recovery = 71% Analysis Date = 10/27/15 Pct Recovery = 71% Analysis Date = 10/27/15 Pct Recovery = 71% Analysis Date = 10/22/15 Pct Recovery = 71% Analysis Date = 10/22/15 Pct Recovery = 71% Analysis Date = 10/17/15 Pct Recovery = 72% Analysis Date = 10/17/15 Pct Recovery = 72% Analysis Date = 10/12/15 Pct Recovery = 72% Analysis Date = 10/12/15 Pct Recovery = 72% Analysis Date = 10/07/15 Pct Recovery = 72% Analysis Date = 10/07/15 Pct Recovery = 72% Analysis Date = 10/02/15 Pct Recovery = 72% Analysis Date = 10/02/15 Pct Recovery = 72% Analysis Date = 09/27/15 Pct Recovery = 72% Analysis Date = 09/27/15 Pct Recovery = 72% Analysis Date = 09/22/15 Pct Recovery = 72% Analysis Date = 09/22/15 Pct Recovery = 72% Analysis Date = 09/17/15 Pct Recovery = 73% Analysis Date = 09/17/15 Pct Recovery = 73% Analysis Date = 09/13/15 Pct Recovery = 73% Analysis Date = 09/13/15 Pct Recovery = 73% Analysis Date = 09/08/15 Pct Recovery = 73% Analysis Date = 09/08/15 Pct Recovery = 73% Analysis Date = 09/03/15 Pct Recovery = 73% Analysis Date = 09/03/15 Pct Recovery = 73% Analysis Date = 08/29/15 Pct Recovery = 73% Analysis Date = 08/29/15 Pct Recovery = 73% Analysis Date = 08/24/15 Pct Recovery = 73% Analysis Date = 08/24/15 Pct Recovery = 73% Analysis Date = 08/19/15 Pct Recovery = 74% Analysis Date = 08/19/15 Pct Recovery = 74% Analysis Date = 08/14/15 Pct Recovery = 74% Analysis Date = 08/14/15 Pct Recovery = 74% Analysis Date = 08/09/15 Pct Recovery = 74% Analysis Date = 08/09/15 Pct Recovery = 74% Analysis Date = 08/04/15 Pct Recovery = 74% Analysis Date = 08/04/15 Pct Recovery = 74% Analysis Date = 07/31/15 Pct Recovery = 74% Analysis Date = 07/31/15 Pct Recovery = 74% Analysis Date = 07/26/15 Pct Recovery = 74% Analysis Date = 07/26/15 Pct Recovery = 74% Analysis Date = 07/21/15 Pct Recovery = 74% Analysis Date = 07/21/15 Pct Recovery = 74% Analysis Date = 07/16/15 Pct Recovery = 74% Analysis Date = 07/16/15 Pct Recovery = 74% Analysis Date = 07/11/15 Pct Recovery = 74% Analysis Date = 07/11/15 Pct Recovery = 74% Analysis Date = 07/06/15 Pct Recovery = 74% Analysis Date = 07/06/15 Pct Recovery = 74% Analysis Date = 07/01/15 Pct Recovery = 74% Analysis Date = 07/01/15 Pct Recovery = 74% Analysis Date = 06/26/15 Pct Recovery = 74% Analysis Date = 06/26/15 Pct Recovery = 74% Analysis Date = 06/21/15 Pct Recovery = 74% Analysis Date = 06/21/15 Pct Recovery = 74% Analysis Date = 06/17/15 Pct Recovery = 74% Analysis Date = 06/17/15 Pct Recovery = 74% Analysis Date = 06/12/15 Pct Recovery = 74% Analysis Date = 06/12/15 Pct Recovery = 74% Analysis Date = 06/07/15 Pct Recovery = 74% Analysis Date = 06/07/15 Pct Recovery = 74% Analysis Date = 06/02/15 Pct Recovery = 74% Analysis Date = 06/02/15 Pct Recovery = 74% Analysis Date = 05/28/15 Pct Recovery = 74% Analysis Date = 05/28/15 Pct Recovery = 74% Analysis Date = 05/23/15 Pct Recovery = 74% Analysis Date = 05/23/15 Pct Recovery = 74% Analysis Date = 05/18/15 Pct Recovery = 74% Analysis Date = 05/18/15 Pct Recovery = 74% Analysis Date = 05/13/15 Pct Recovery = 74% Analysis Date = 05/13/15 Pct Recovery = 74% Analysis Date = 05/08/15 Pct Recovery = 74% Analysis Date = 05/08/15 Pct Recovery = 74% Analysis Date = 05/04/15 Pct Recovery = 74% Analysis Date = 05/04/15 Pct Recovery = 74% Analysis Date = 04/29/15 Pct Recovery = 74% Analysis Date = 04/29/15 Pct Recovery = 74% Analysis Date = 04/24/15 Pct Recovery = 74% Analysis Date = 04/24/15 Pct Recovery = 74% Analysis Date = 04/19/15 Pct Recovery = 74% Analysis Date = 04/19/15 Pct Recovery = 74% Analysis Date = 04/14/15 Pct Recovery = 74% Analysis Date = 04/14/15 Pct Recovery = 74% Analysis Date = 04/09/15 Pct Recovery = 74% Analysis Date = 04/09/15 Pct Recovery = 74% Analysis Date = 04/04/15 Pct Recovery = 74% Analysis Date = 04/04/15 Pct Recovery = 74% Analysis Date = 03/30/15 Pct Recovery = 74% Analysis Date = 03/30/15 Pct Recovery = 74% Analysis Date = 03/25/15 Pct Recovery = 74% Analysis Date = 03/25/15 Pct Recovery = 74% Analysis Date = 03/21/15 Pct Recovery = 74% Analysis Date = 03/21/15 Pct Recovery = 74% Analysis Date = 03/16/15 Pct Recovery = 74% Analysis Date = 03/16/15 Pct Recovery = 74% Analysis Date = 03/11/15 Pct Recovery = 74% Analysis Date = 03/11/15 Pct Recovery = 74% Analysis Date = 03/06/15 Pct Recovery = 74% Analysis Date = 03/06/15 Pct Recovery = 74% Analysis Date = 03/01/15 Pct Recovery = 74% Analysis Date = 03/01/15 Pct Recovery = 74% Analysis Date = 02/24/15 Pct Recovery = 74% Analysis Date = 02/24/15 Pct Recovery = 74% Analysis Date = 02/19/15 Pct Recovery = 74% Analysis Date = 02/19/15 Pct Recovery = 74% Analysis Date = 02/14/15 Pct Recovery = 74% Analysis Date = 02/14/15 Pct Recovery = 74% Analysis Date = 02/09/15 Pct Recovery = 74% Analysis Date = 02/09/15 Pct Recovery = 74% Analysis Date = 02/05/15 Pct Recovery = 74% Analysis Date = 02/05/15 Pct Recovery = 74% Analysis Date = 01/31/15 Pct Recovery = 74% Analysis Date = 01/31/15 Pct Recovery = 74% Analysis Date = 01/26/15 Pct Recovery = 74% Analysis Date = 01/26/15 Pct Recovery = 74% Analysis Date = 01/21/15 Pct Recovery = 74% Analysis Date = 01/21/15 Pct Recovery = 74% Analysis Date = 01/16/15 Pct Recovery = 74% Analysis Date = 01/16/15 Pct Recovery = 74% Analysis Date = 01/11/15 Pct Recovery = 74% Analysis Date = 01/11/15 Pct Recovery = 74% Analysis Date = 01/06/15 Pct Recovery = 74% Analysis Date = 01/06/15 Pct Recovery = 74% Analysis Date = 01/01/15 Pct Recovery = 74% Analysis Date = 01/01/15 Pct Recovery = 74% Analysis Date = 12/27/14 Pct Recovery = 74% Analysis Date = 12/27/14 Pct Recovery = 74% Analysis Date = 12/23/14 Pct Recovery = 74% Analysis Date = 12/23/14 Pct Recovery = 74% Analysis Date = 12/18/14 Pct Recovery = 74% Analysis Date = 12/18/14 Pct Recovery = 74% Analysis Date = 12/13/14 Pct Recovery = 74% Analysis Date = 12/13/14 Pct Recovery = 74% Analysis Date = 12/08/14 Pct Recovery = 74% Analysis Date = 12/08/14 Pct Recovery = 74% Analysis Date = 12/03/14 Pct Recovery = 74% Analysis Date = 12/03/14 Pct Recovery = 74% Analysis Date = 11/28/14 Pct Recovery = 74% Analysis Date = 11/28/14 Pct Recovery = 74% Analysis Date = 11/23/14 Pct Recovery = 74% Analysis Date = 11/23/14 Pct Recovery = 74% Analysis Date = 11/18/14 Pct Recovery = 74% Analysis Date = 11/18/14 Pct Recovery = 74% Analysis Date = 11/13/14 Pct Recovery = 74% Analysis Date = 11/13/14 Pct Recovery = 74% Analysis Date = 11/09/14 Pct Recovery = 74% Analysis Date = 11/09/14 Pct Recovery = 74% Analysis Date = 11/04/14 Pct Recovery = 74% Analysis Date = 11/04/14 Pct Recovery = 74% Analysis Date = 10/30/14 Pct Recovery = 74% Analysis Date = 10/30/14 Pct Recovery = 74% Analysis Date = 10/25/14 Pct Recovery = 74% Analysis Date = 10/25/14 Pct Recovery = 74% Analysis Date = 10/20/14 Pct Recovery = 74% Analysis Date = 10/20/14 Pct Recovery = 74% Analysis Date = 10/15/14 Pct Recovery = 74% Analysis Date = 10/15/14 Pct Recovery = 74% Analysis Date = 10/10/14 Pct Recovery = 74% Analysis Date = 10/10/14 Pct Recovery = 74% Analysis Date = 10/05/14 Pct Recovery = 74% Analysis Date = 10/05/14 Pct Recovery = 74% Analysis Date = 09/30/14 Pct Recovery = 74% Analysis Date = 09/30/14 Pct Recovery = 74% Analysis Date = 09/26/14 Pct Recovery = 74% Analysis Date = 09/26/14 Pct Recovery = 74% Analysis Date = 09/21/14 Pct Recovery = 74% Analysis Date = 09/21/14 Pct Recovery = 74% Analysis Date = 09/16/14 Pct Recovery = 74% Analysis Date = 09/16/14 Pct Recovery = 74% Analysis Date = 09/11/14 Pct Recovery = 74% Analysis Date = 09/11/14 Pct Recovery = 74% Analysis Date = 09/06/14 Pct Recovery = 74% Analysis Date = 09/06/14 Pct Recovery = 74% Analysis Date = 09/01/14 Pct Recovery = 74% Analysis Date = 09/01/14 Pct Recovery = 74% Analysis Date = 08/27/14 Pct Recovery = 74% Analysis Date = 08/27/14 Pct Recovery = 74% Analysis Date = 08/22/14 Pct Recovery = 74% Analysis Date = 08/22/14 Pct Recovery = 74% Analysis Date = 08/17/14 Pct Recovery = 74% Analysis Date = 08/17/14 Pct Recovery = 74% Analysis Date = 08/13/14 Pct Recovery = 74% Analysis Date = 08/13/14 Pct Recovery = 74% Analysis Date = 08/08/14 Pct Recovery = 74% Analysis Date = 08/08/14 Pct Recovery = 74% Analysis Date = 08/03/14 Pct Recovery = 74% Analysis Date = 08/03/14 Pct Recovery = 74% Analysis Date = 07/29/14 Pct Recovery = 74% Analysis Date = 07/29/14 Pct Recovery = 74% Analysis Date = 07/24/14 Pct Recovery = 74% Analysis Date = 07/24/14 Pct Recovery = 74% Analysis Date = 07/19/14 Pct Recovery = 74% Analysis Date = 07/19/14 Pct Recovery = 74% Analysis Date = 07/14/14 Pct Recovery = 74% Analysis Date = 07/14/14 Pct Recovery = 74% Analysis Date = 07/09/14 Pct Recovery = 74% Analysis Date = 07/09/14 Pct Recovery = 74% Analysis Date = 07/04/14 Pct Recovery = 74% Analysis Date = 07/04/14 Pct Recovery = 74% Analysis Date = 06/30/14 Pct Recovery = 74% Analysis Date = 06/30/14 Pct Recovery = 74% Analysis Date = 06/25/14 Pct Recovery = 74% Analysis Date = 06/25/14 Pct Recovery = 74% Analysis Date = 06/20/14 Pct Recovery = 74% Analysis Date = 06/20/14 Pct Recovery = 74% Analysis Date = 06/15/14 Pct Recovery = 74% Analysis Date = 06/15/14 Pct Recovery = 74% Analysis Date = 06/10/14 Pct Recovery = 74% Analysis Date = 06/10/14 Pct Recovery = 74% Analysis Date = 06/05/14 Pct Recovery = 74% Analysis Date = 06/05/14 Pct Recovery = 74% Analysis Date = 05/31/14 Pct Recovery = 74% Analysis Date = 05/31/14 Pct Recovery = 74% Analysis Date = 05/26/14 Pct Recovery = 74% Analysis Date = 05/26/14 Pct Recovery = 74% Analysis Date = 05/21/14 Pct Recovery = 74% Analysis Date = 05/21/14 Pct Recovery = 74% Analysis Date = 05/17/14 Pct Recovery = 74% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
CODEINE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 51 82% 18% 81% 16%
Total 51 82% 18% 81% 16%

Sample Statistics
CODEINE

Characteristic N % % Basis
Plotted 51 100% Spiked
Estimated Values 6 12% Spiked
Deleted Values 2 2% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 51 .  
False Negatives 0 0% 0 out of 51
Not Spiked 64 .  
False Positives 0 0% 0 out of 62

BQS OBSP Determination:
COTININE
METHOD: 2440 , TESTIDCODE: 67444LCM56
Open Data Set

Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 80% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 74% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 80 µl & ERA 0406-15-08: 80 µl Pct Recovery = 86% Analysis Date = 11/04/15 SpikeMix = Abs 052215: 80 µl & Abs 050115: 80 µl Pct Recovery = 86% Analysis Date = 01/17/16 SpikeMix = ERA 0406-15-09: 80 µl & ERA 0406-15-07A: 80 µl Pct Recovery = 57% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 80 µl & Abs 051315: 80 µl Pct Recovery = 69% Analysis Date = 09/24/16 SpikeMix = Crescent EN160610015: 80 µl & Abs 061416: 80 µl Pct Recovery = 89% Analysis Date = 09/24/16 SpikeMix = Abs 061416: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 86% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 98% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 92% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 92% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 94% Analysis Date = 11/18/16 SpikeMix = ERA 04281604: 80 µl & ERA 04281603: 80 µl Pct Recovery = 75% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & ERA 04281604: 80 µl Pct Recovery = 73% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-04: 15 µl & Abs 041814: 15 µl Pct Recovery = 77% Analysis Date = 02/06/15 SpikeMix = Abs 041814: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 79% Analysis Date = 07/12/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 91% Analysis Date = 06/22/14 SpikeMix = Abs 041814: 60 µl & Abs 041614: 60 µl Pct Recovery = 105% Analysis Date = 05/21/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 86% Analysis Date = 05/07/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 98% Analysis Date = 04/29/15 SpikeMix = ERA 0319-14-05: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 93% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 79% Analysis Date = 01/16/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 87% Analysis Date = 12/07/14 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 80% Analysis Date = 12/06/14 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 74% Analysis Date = 08/28/14 SpikeMix = ERA 0319-14-04: 60 µl & ERA 0319-14-05: 60 µl Pct Recovery = 65% Analysis Date = 07/26/14 SpikeMix = ERA 0319-14-05: 60 µl & ERA 0318-14-02: 60 µl Pct Recovery = 107% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 80% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 71% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 80% Analysis Date = 02/23/16 SpikeMix = Abs 052215: 40 µl & Abs 050115: 40 µl Pct Recovery = 78% Analysis Date = 07/31/15 SpikeMix = ERA 0406-15-09: 40 µl & Abs 050115: 40 µl Pct Recovery = 104% Analysis Date = 07/30/15 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 75% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-07A: 40 µl & Abs 051315: 40 µl Pct Recovery = 64% Analysis Date = 11/04/15 SpikeMix = ERA 0406-15-07A: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 63% Analysis Date = 09/10/15 SpikeMix = Abs 052215: 40 µl & ERA 0406-15-07A: 40 µl Pct Recovery = 63% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 79% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 97% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 81% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 88% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 73% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 78% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 76% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 75% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 95% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 104% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 80% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 79% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 70% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 67% Analysis Date = 04/23/14 SpikeMix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.2: 20 µl Pct Recovery = 93% Analysis Date = 04/10/15 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 84% Analysis Date = 11/04/14 SpikeMix = Abs 041814: 8 µl & ERA 0318-14-02: 8 µl Pct Recovery = 66% Analysis Date = 10/11/14 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 61% Analysis Date = 11/04/14 SpikeMix = Abs 041714: 8 µl & ERA 0319-14-05: 8 µl Pct Recovery = 76% Analysis Date = 10/24/14 SpikeMix = ERA 0319-14-05: 8 µl & Abs 041614: 8 µl Pct Recovery = 91% Analysis Date = 10/10/14 SpikeMix = Abs 041714: 30 µl & Abs 041814: 30 µl Pct Recovery = 73% Analysis Date = 10/10/14 SpikeMix = Abs 041814: 30 µl & ERA 0318-14-02: 30 µl Pct Recovery = 62% Analysis Date = 07/13/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 94% Analysis Date = 05/30/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 88% Analysis Date = 08/30/14 SpikeMix = ERA 0318-14-02: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 89% Analysis Date = 08/16/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 56% Analysis Date = 11/25/15 SpikeMix = Abs 050115: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 93% Analysis Date = 11/24/15 SpikeMix = ERA 0406-15-09: 20 µl & Abs 050115: 20 µl Pct Recovery = 95% Analysis Date = 08/27/15 SpikeMix = Abs 052215: 20 µl & Abs 050115: 20 µl Pct Recovery = 83% Analysis Date = 08/13/15 SpikeMix = Abs 050115: 20 µl & Abs 051315: 20 µl Pct Recovery = 58% Analysis Date = 07/09/15 SpikeMix = Abs 050115: 20 µl & Abs 052215: 20 µl Pct Recovery = 81% Analysis Date = 06/09/15 SpikeMix = Abs 051315: 20 µl & Abs 050115: 20 µl Pct Recovery = 62% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 67% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 53% Analysis Date = 04/27/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 98% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 81% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 58% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 56% Analysis Date = 11/24/15 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 78% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-09: 20 µl Pct Recovery = 54% Analysis Date = 01/04/17 Pct Recovery = 87% Analysis Date = 12/31/16 Pct Recovery = 86% Analysis Date = 12/31/16 Pct Recovery = 86% Analysis Date = 12/26/16 Pct Recovery = 86% Analysis Date = 12/26/16 Pct Recovery = 86% Analysis Date = 12/21/16 Pct Recovery = 86% Analysis Date = 12/21/16 Pct Recovery = 86% Analysis Date = 12/16/16 Pct Recovery = 86% Analysis Date = 12/16/16 Pct Recovery = 86% Analysis Date = 12/11/16 Pct Recovery = 85% Analysis Date = 12/11/16 Pct Recovery = 85% Analysis Date = 12/06/16 Pct Recovery = 85% Analysis Date = 12/06/16 Pct Recovery = 85% Analysis Date = 12/01/16 Pct Recovery = 85% Analysis Date = 12/01/16 Pct Recovery = 85% Analysis Date = 11/26/16 Pct Recovery = 85% Analysis Date = 11/26/16 Pct Recovery = 85% Analysis Date = 11/21/16 Pct Recovery = 85% Analysis Date = 11/21/16 Pct Recovery = 85% Analysis Date = 11/16/16 Pct Recovery = 84% Analysis Date = 11/16/16 Pct Recovery = 84% Analysis Date = 11/11/16 Pct Recovery = 84% Analysis Date = 11/11/16 Pct Recovery = 84% Analysis Date = 11/06/16 Pct Recovery = 84% Analysis Date = 11/06/16 Pct Recovery = 84% Analysis Date = 11/01/16 Pct Recovery = 84% Analysis Date = 11/01/16 Pct Recovery = 84% Analysis Date = 10/27/16 Pct Recovery = 84% Analysis Date = 10/27/16 Pct Recovery = 84% Analysis Date = 10/22/16 Pct Recovery = 83% Analysis Date = 10/22/16 Pct Recovery = 83% Analysis Date = 10/17/16 Pct Recovery = 83% Analysis Date = 10/17/16 Pct Recovery = 83% Analysis Date = 10/13/16 Pct Recovery = 83% Analysis Date = 10/13/16 Pct Recovery = 83% Analysis Date = 10/08/16 Pct Recovery = 83% Analysis Date = 10/08/16 Pct Recovery = 83% Analysis Date = 10/03/16 Pct Recovery = 82% Analysis Date = 10/03/16 Pct Recovery = 82% Analysis Date = 09/28/16 Pct Recovery = 82% Analysis Date = 09/28/16 Pct Recovery = 82% Analysis Date = 09/23/16 Pct Recovery = 82% Analysis Date = 09/23/16 Pct Recovery = 82% Analysis Date = 09/18/16 Pct Recovery = 82% Analysis Date = 09/18/16 Pct Recovery = 82% Analysis Date = 09/13/16 Pct Recovery = 82% Analysis Date = 09/13/16 Pct Recovery = 82% Analysis Date = 09/08/16 Pct Recovery = 81% Analysis Date = 09/08/16 Pct Recovery = 81% Analysis Date = 09/03/16 Pct Recovery = 81% Analysis Date = 09/03/16 Pct Recovery = 81% Analysis Date = 08/29/16 Pct Recovery = 81% Analysis Date = 08/29/16 Pct Recovery = 81% Analysis Date = 08/24/16 Pct Recovery = 81% Analysis Date = 08/24/16 Pct Recovery = 81% Analysis Date = 08/19/16 Pct Recovery = 80% Analysis Date = 08/19/16 Pct Recovery = 80% Analysis Date = 08/14/16 Pct Recovery = 80% Analysis Date = 08/14/16 Pct Recovery = 80% Analysis Date = 08/09/16 Pct Recovery = 80% Analysis Date = 08/09/16 Pct Recovery = 80% Analysis Date = 08/04/16 Pct Recovery = 80% Analysis Date = 08/04/16 Pct Recovery = 80% Analysis Date = 07/30/16 Pct Recovery = 80% Analysis Date = 07/30/16 Pct Recovery = 80% Analysis Date = 07/25/16 Pct Recovery = 80% Analysis Date = 07/25/16 Pct Recovery = 80% Analysis Date = 07/21/16 Pct Recovery = 80% Analysis Date = 07/21/16 Pct Recovery = 80% Analysis Date = 07/16/16 Pct Recovery = 79% Analysis Date = 07/16/16 Pct Recovery = 79% Analysis Date = 07/11/16 Pct Recovery = 79% Analysis Date = 07/11/16 Pct Recovery = 79% Analysis Date = 07/06/16 Pct Recovery = 79% Analysis Date = 07/06/16 Pct Recovery = 79% Analysis Date = 07/01/16 Pct Recovery = 79% Analysis Date = 07/01/16 Pct Recovery = 79% Analysis Date = 06/26/16 Pct Recovery = 79% Analysis Date = 06/26/16 Pct Recovery = 79% Analysis Date = 06/21/16 Pct Recovery = 79% Analysis Date = 06/21/16 Pct Recovery = 79% Analysis Date = 06/16/16 Pct Recovery = 78% Analysis Date = 06/16/16 Pct Recovery = 78% Analysis Date = 06/11/16 Pct Recovery = 78% Analysis Date = 06/11/16 Pct Recovery = 78% Analysis Date = 06/06/16 Pct Recovery = 78% Analysis Date = 06/06/16 Pct Recovery = 78% Analysis Date = 06/01/16 Pct Recovery = 78% Analysis Date = 06/01/16 Pct Recovery = 78% Analysis Date = 05/27/16 Pct Recovery = 78% Analysis Date = 05/27/16 Pct Recovery = 78% Analysis Date = 05/22/16 Pct Recovery = 78% Analysis Date = 05/22/16 Pct Recovery = 78% Analysis Date = 05/17/16 Pct Recovery = 78% Analysis Date = 05/17/16 Pct Recovery = 78% Analysis Date = 05/12/16 Pct Recovery = 77% Analysis Date = 05/12/16 Pct Recovery = 77% Analysis Date = 05/07/16 Pct Recovery = 77% Analysis Date = 05/07/16 Pct Recovery = 77% Analysis Date = 05/02/16 Pct Recovery = 77% Analysis Date = 05/02/16 Pct Recovery = 77% Analysis Date = 04/28/16 Pct Recovery = 77% Analysis Date = 04/28/16 Pct Recovery = 77% Analysis Date = 04/23/16 Pct Recovery = 77% Analysis Date = 04/23/16 Pct Recovery = 77% Analysis Date = 04/18/16 Pct Recovery = 77% Analysis Date = 04/18/16 Pct Recovery = 77% Analysis Date = 04/13/16 Pct Recovery = 77% Analysis Date = 04/13/16 Pct Recovery = 77% Analysis Date = 04/08/16 Pct Recovery = 76% Analysis Date = 04/08/16 Pct Recovery = 76% Analysis Date = 04/03/16 Pct Recovery = 76% Analysis Date = 04/03/16 Pct Recovery = 76% Analysis Date = 03/29/16 Pct Recovery = 76% Analysis Date = 03/29/16 Pct Recovery = 76% Analysis Date = 03/24/16 Pct Recovery = 76% Analysis Date = 03/24/16 Pct Recovery = 76% Analysis Date = 03/19/16 Pct Recovery = 76% Analysis Date = 03/19/16 Pct Recovery = 76% Analysis Date = 03/14/16 Pct Recovery = 76% Analysis Date = 03/14/16 Pct Recovery = 76% Analysis Date = 03/09/16 Pct Recovery = 76% Analysis Date = 03/09/16 Pct Recovery = 76% Analysis Date = 03/04/16 Pct Recovery = 76% Analysis Date = 03/04/16 Pct Recovery = 76% Analysis Date = 02/28/16 Pct Recovery = 76% Analysis Date = 02/28/16 Pct Recovery = 76% Analysis Date = 02/23/16 Pct Recovery = 75% Analysis Date = 02/23/16 Pct Recovery = 75% Analysis Date = 02/18/16 Pct Recovery = 75% Analysis Date = 02/18/16 Pct Recovery = 75% Analysis Date = 02/13/16 Pct Recovery = 75% Analysis Date = 02/13/16 Pct Recovery = 75% Analysis Date = 02/09/16 Pct Recovery = 75% Analysis Date = 02/09/16 Pct Recovery = 75% Analysis Date = 02/04/16 Pct Recovery = 75% Analysis Date = 02/04/16 Pct Recovery = 75% Analysis Date = 01/30/16 Pct Recovery = 75% Analysis Date = 01/30/16 Pct Recovery = 75% Analysis Date = 01/25/16 Pct Recovery = 75% Analysis Date = 01/25/16 Pct Recovery = 75% Analysis Date = 01/20/16 Pct Recovery = 75% Analysis Date = 01/20/16 Pct Recovery = 75% Analysis Date = 01/15/16 Pct Recovery = 75% Analysis Date = 01/15/16 Pct Recovery = 75% Analysis Date = 01/10/16 Pct Recovery = 75% Analysis Date = 01/10/16 Pct Recovery = 75% Analysis Date = 01/05/16 Pct Recovery = 75% Analysis Date = 01/05/16 Pct Recovery = 75% Analysis Date = 12/31/15 Pct Recovery = 75% Analysis Date = 12/31/15 Pct Recovery = 75% Analysis Date = 12/26/15 Pct Recovery = 75% Analysis Date = 12/26/15 Pct Recovery = 75% Analysis Date = 12/21/15 Pct Recovery = 75% Analysis Date = 12/21/15 Pct Recovery = 75% Analysis Date = 12/16/15 Pct Recovery = 75% Analysis Date = 12/16/15 Pct Recovery = 75% Analysis Date = 12/11/15 Pct Recovery = 75% Analysis Date = 12/11/15 Pct Recovery = 75% Analysis Date = 12/06/15 Pct Recovery = 75% Analysis Date = 12/06/15 Pct Recovery = 75% Analysis Date = 12/01/15 Pct Recovery = 75% Analysis Date = 12/01/15 Pct Recovery = 75% Analysis Date = 11/26/15 Pct Recovery = 75% Analysis Date = 11/26/15 Pct Recovery = 75% Analysis Date = 11/21/15 Pct Recovery = 75% Analysis Date = 11/21/15 Pct Recovery = 75% Analysis Date = 11/17/15 Pct Recovery = 75% Analysis Date = 11/17/15 Pct Recovery = 75% Analysis Date = 11/12/15 Pct Recovery = 75% Analysis Date = 11/12/15 Pct Recovery = 75% Analysis Date = 11/07/15 Pct Recovery = 75% Analysis Date = 11/07/15 Pct Recovery = 75% Analysis Date = 11/02/15 Pct Recovery = 76% Analysis Date = 11/02/15 Pct Recovery = 76% Analysis Date = 10/28/15 Pct Recovery = 76% Analysis Date = 10/28/15 Pct Recovery = 76% Analysis Date = 10/23/15 Pct Recovery = 76% Analysis Date = 10/23/15 Pct Recovery = 76% Analysis Date = 10/18/15 Pct Recovery = 76% Analysis Date = 10/18/15 Pct Recovery = 76% Analysis Date = 10/13/15 Pct Recovery = 76% Analysis Date = 10/13/15 Pct Recovery = 76% Analysis Date = 10/08/15 Pct Recovery = 76% Analysis Date = 10/08/15 Pct Recovery = 76% Analysis Date = 10/03/15 Pct Recovery = 76% Analysis Date = 10/03/15 Pct Recovery = 76% Analysis Date = 09/28/15 Pct Recovery = 76% Analysis Date = 09/28/15 Pct Recovery = 76% Analysis Date = 09/23/15 Pct Recovery = 76% Analysis Date = 09/23/15 Pct Recovery = 76% Analysis Date = 09/18/15 Pct Recovery = 76% Analysis Date = 09/18/15 Pct Recovery = 76% Analysis Date = 09/13/15 Pct Recovery = 77% Analysis Date = 09/13/15 Pct Recovery = 77% Analysis Date = 09/08/15 Pct Recovery = 77% Analysis Date = 09/08/15 Pct Recovery = 77% Analysis Date = 09/03/15 Pct Recovery = 77% Analysis Date = 09/03/15 Pct Recovery = 77% Analysis Date = 08/29/15 Pct Recovery = 77% Analysis Date = 08/29/15 Pct Recovery = 77% Analysis Date = 08/25/15 Pct Recovery = 77% Analysis Date = 08/25/15 Pct Recovery = 77% Analysis Date = 08/20/15 Pct Recovery = 77% Analysis Date = 08/20/15 Pct Recovery = 77% Analysis Date = 08/15/15 Pct Recovery = 77% Analysis Date = 08/15/15 Pct Recovery = 77% Analysis Date = 08/10/15 Pct Recovery = 77% Analysis Date = 08/10/15 Pct Recovery = 77% Analysis Date = 08/05/15 Pct Recovery = 77% Analysis Date = 08/05/15 Pct Recovery = 77% Analysis Date = 07/31/15 Pct Recovery = 77% Analysis Date = 07/31/15 Pct Recovery = 77% Analysis Date = 07/26/15 Pct Recovery = 77% Analysis Date = 07/26/15 Pct Recovery = 77% Analysis Date = 07/21/15 Pct Recovery = 77% Analysis Date = 07/21/15 Pct Recovery = 77% Analysis Date = 07/16/15 Pct Recovery = 77% Analysis Date = 07/16/15 Pct Recovery = 77% Analysis Date = 07/11/15 Pct Recovery = 77% Analysis Date = 07/11/15 Pct Recovery = 77% Analysis Date = 07/06/15 Pct Recovery = 77% Analysis Date = 07/06/15 Pct Recovery = 77% Analysis Date = 07/01/15 Pct Recovery = 77% Analysis Date = 07/01/15 Pct Recovery = 77% Analysis Date = 06/26/15 Pct Recovery = 77% Analysis Date = 06/26/15 Pct Recovery = 77% Analysis Date = 06/21/15 Pct Recovery = 77% Analysis Date = 06/21/15 Pct Recovery = 77% Analysis Date = 06/16/15 Pct Recovery = 77% Analysis Date = 06/16/15 Pct Recovery = 77% Analysis Date = 06/11/15 Pct Recovery = 77% Analysis Date = 06/11/15 Pct Recovery = 77% Analysis Date = 06/07/15 Pct Recovery = 77% Analysis Date = 06/07/15 Pct Recovery = 77% Analysis Date = 06/02/15 Pct Recovery = 78% Analysis Date = 06/02/15 Pct Recovery = 78% Analysis Date = 05/28/15 Pct Recovery = 78% Analysis Date = 05/28/15 Pct Recovery = 78% Analysis Date = 05/23/15 Pct Recovery = 78% Analysis Date = 05/23/15 Pct Recovery = 78% Analysis Date = 05/18/15 Pct Recovery = 78% Analysis Date = 05/18/15 Pct Recovery = 78% Analysis Date = 05/13/15 Pct Recovery = 78% Analysis Date = 05/13/15 Pct Recovery = 78% Analysis Date = 05/08/15 Pct Recovery = 78% Analysis Date = 05/08/15 Pct Recovery = 78% Analysis Date = 05/03/15 Pct Recovery = 78% Analysis Date = 05/03/15 Pct Recovery = 78% Analysis Date = 04/28/15 Pct Recovery = 78% Analysis Date = 04/28/15 Pct Recovery = 78% Analysis Date = 04/23/15 Pct Recovery = 78% Analysis Date = 04/23/15 Pct Recovery = 78% Analysis Date = 04/18/15 Pct Recovery = 78% Analysis Date = 04/18/15 Pct Recovery = 78% Analysis Date = 04/13/15 Pct Recovery = 78% Analysis Date = 04/13/15 Pct Recovery = 78% Analysis Date = 04/08/15 Pct Recovery = 78% Analysis Date = 04/08/15 Pct Recovery = 78% Analysis Date = 04/03/15 Pct Recovery = 78% Analysis Date = 04/03/15 Pct Recovery = 78% Analysis Date = 03/29/15 Pct Recovery = 78% Analysis Date = 03/29/15 Pct Recovery = 78% Analysis Date = 03/24/15 Pct Recovery = 78% Analysis Date = 03/24/15 Pct Recovery = 78% Analysis Date = 03/19/15 Pct Recovery = 78% Analysis Date = 03/19/15 Pct Recovery = 78% Analysis Date = 03/15/15 Pct Recovery = 78% Analysis Date = 03/15/15 Pct Recovery = 78% Analysis Date = 03/10/15 Pct Recovery = 79% Analysis Date = 03/10/15 Pct Recovery = 79% Analysis Date = 03/05/15 Pct Recovery = 79% Analysis Date = 03/05/15 Pct Recovery = 79% Analysis Date = 02/28/15 Pct Recovery = 79% Analysis Date = 02/28/15 Pct Recovery = 79% Analysis Date = 02/23/15 Pct Recovery = 79% Analysis Date = 02/23/15 Pct Recovery = 79% Analysis Date = 02/18/15 Pct Recovery = 79% Analysis Date = 02/18/15 Pct Recovery = 79% Analysis Date = 02/13/15 Pct Recovery = 79% Analysis Date = 02/13/15 Pct Recovery = 79% Analysis Date = 02/08/15 Pct Recovery = 79% Analysis Date = 02/08/15 Pct Recovery = 79% Analysis Date = 02/03/15 Pct Recovery = 79% Analysis Date = 02/03/15 Pct Recovery = 79% Analysis Date = 01/29/15 Pct Recovery = 79% Analysis Date = 01/29/15 Pct Recovery = 79% Analysis Date = 01/24/15 Pct Recovery = 79% Analysis Date = 01/24/15 Pct Recovery = 79% Analysis Date = 01/19/15 Pct Recovery = 79% Analysis Date = 01/19/15 Pct Recovery = 79% Analysis Date = 01/14/15 Pct Recovery = 80% Analysis Date = 01/14/15 Pct Recovery = 80% Analysis Date = 01/09/15 Pct Recovery = 80% Analysis Date = 01/09/15 Pct Recovery = 80% Analysis Date = 01/04/15 Pct Recovery = 80% Analysis Date = 01/04/15 Pct Recovery = 80% Analysis Date = 12/30/14 Pct Recovery = 80% Analysis Date = 12/30/14 Pct Recovery = 80% Analysis Date = 12/25/14 Pct Recovery = 80% Analysis Date = 12/25/14 Pct Recovery = 80% Analysis Date = 12/21/14 Pct Recovery = 80% Analysis Date = 12/21/14 Pct Recovery = 80% Analysis Date = 12/16/14 Pct Recovery = 80% Analysis Date = 12/16/14 Pct Recovery = 80% Analysis Date = 12/11/14 Pct Recovery = 80% Analysis Date = 12/11/14 Pct Recovery = 80% Analysis Date = 12/06/14 Pct Recovery = 80% Analysis Date = 12/06/14 Pct Recovery = 80% Analysis Date = 12/01/14 Pct Recovery = 81% Analysis Date = 12/01/14 Pct Recovery = 81% Analysis Date = 11/26/14 Pct Recovery = 81% Analysis Date = 11/26/14 Pct Recovery = 81% Analysis Date = 11/21/14 Pct Recovery = 81% Analysis Date = 11/21/14 Pct Recovery = 81% Analysis Date = 11/16/14 Pct Recovery = 81% Analysis Date = 11/16/14 Pct Recovery = 81% Analysis Date = 11/11/14 Pct Recovery = 81% Analysis Date = 11/11/14 Pct Recovery = 81% Analysis Date = 11/06/14 Pct Recovery = 81% Analysis Date = 11/06/14 Pct Recovery = 81% Analysis Date = 11/01/14 Pct Recovery = 81% Analysis Date = 11/01/14 Pct Recovery = 81% Analysis Date = 10/27/14 Pct Recovery = 81% Analysis Date = 10/27/14 Pct Recovery = 81% Analysis Date = 10/22/14 Pct Recovery = 82% Analysis Date = 10/22/14 Pct Recovery = 82% Analysis Date = 10/17/14 Pct Recovery = 82% Analysis Date = 10/17/14 Pct Recovery = 82% Analysis Date = 10/12/14 Pct Recovery = 82% Analysis Date = 10/12/14 Pct Recovery = 82% Analysis Date = 10/07/14 Pct Recovery = 82% Analysis Date = 10/07/14 Pct Recovery = 82% Analysis Date = 10/03/14 Pct Recovery = 82% Analysis Date = 10/03/14 Pct Recovery = 82% Analysis Date = 09/28/14 Pct Recovery = 82% Analysis Date = 09/28/14 Pct Recovery = 82% Analysis Date = 09/23/14 Pct Recovery = 82% Analysis Date = 09/23/14 Pct Recovery = 82% Analysis Date = 09/18/14 Pct Recovery = 82% Analysis Date = 09/18/14 Pct Recovery = 82% Analysis Date = 09/13/14 Pct Recovery = 82% Analysis Date = 09/13/14 Pct Recovery = 82% Analysis Date = 09/08/14 Pct Recovery = 83% Analysis Date = 09/08/14 Pct Recovery = 83% Analysis Date = 09/03/14 Pct Recovery = 83% Analysis Date = 09/03/14 Pct Recovery = 83% Analysis Date = 08/29/14 Pct Recovery = 83% Analysis Date = 08/29/14 Pct Recovery = 83% Analysis Date = 08/24/14 Pct Recovery = 83% Analysis Date = 08/24/14 Pct Recovery = 83% Analysis Date = 08/19/14 Pct Recovery = 83% Analysis Date = 08/19/14 Pct Recovery = 83% Analysis Date = 08/14/14 Pct Recovery = 83% Analysis Date = 08/14/14 Pct Recovery = 83% Analysis Date = 08/09/14 Pct Recovery = 83% Analysis Date = 08/09/14 Pct Recovery = 83% Analysis Date = 08/04/14 Pct Recovery = 83% Analysis Date = 08/04/14 Pct Recovery = 83% Analysis Date = 07/30/14 Pct Recovery = 83% Analysis Date = 07/30/14 Pct Recovery = 83% Analysis Date = 07/25/14 Pct Recovery = 84% Analysis Date = 07/25/14 Pct Recovery = 84% Analysis Date = 07/20/14 Pct Recovery = 84% Analysis Date = 07/20/14 Pct Recovery = 84% Analysis Date = 07/15/14 Pct Recovery = 84% Analysis Date = 07/15/14 Pct Recovery = 84% Analysis Date = 07/11/14 Pct Recovery = 84% Analysis Date = 07/11/14 Pct Recovery = 84% Analysis Date = 07/06/14 Pct Recovery = 84% Analysis Date = 07/06/14 Pct Recovery = 84% Analysis Date = 07/01/14 Pct Recovery = 84% Analysis Date = 07/01/14 Pct Recovery = 84% Analysis Date = 06/26/14 Pct Recovery = 84% Analysis Date = 06/26/14 Pct Recovery = 84% Analysis Date = 06/21/14 Pct Recovery = 84% Analysis Date = 06/21/14 Pct Recovery = 84% Analysis Date = 06/16/14 Pct Recovery = 85% Analysis Date = 06/16/14 Pct Recovery = 85% Analysis Date = 06/11/14 Pct Recovery = 85% Analysis Date = 06/11/14 Pct Recovery = 85% Analysis Date = 06/06/14 Pct Recovery = 85% Analysis Date = 06/06/14 Pct Recovery = 85% Analysis Date = 06/01/14 Pct Recovery = 85% Analysis Date = 06/01/14 Pct Recovery = 85% Analysis Date = 05/27/14 Pct Recovery = 85% Analysis Date = 05/27/14 Pct Recovery = 85% Analysis Date = 05/22/14 Pct Recovery = 85% Analysis Date = 05/22/14 Pct Recovery = 85% Analysis Date = 05/17/14 Pct Recovery = 85% Analysis Date = 05/17/14 Pct Recovery = 85% Analysis Date = 05/12/14 Pct Recovery = 85% Analysis Date = 05/12/14 Pct Recovery = 85% Analysis Date = 05/07/14 Pct Recovery = 86% Analysis Date = 05/07/14 Pct Recovery = 86% Analysis Date = 05/02/14 Pct Recovery = 86% Analysis Date = 05/02/14 Pct Recovery = 86% Analysis Date = 04/27/14 Pct Recovery = 86% Analysis Date = 04/27/14 Pct Recovery = 86% Analysis Date = 04/23/14 Pct Recovery = 86% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
COTININE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 76 80% 13% 79% 14%
Total 76 80% 13% 79% 14%

Sample Statistics
COTININE

Characteristic N % % Basis
Plotted 76 97% Spiked
Estimated Values 14 18% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 78 .  
False Negatives 2 3% 2 out of 78
Not Spiked 37 .  
False Positives 4 11% 4 out of 37

BQS OBSP Determination:
DEHYDRONIFEDIPINE
METHOD: 2440 , TESTIDCODE: 67445LCM56
Open Data Set

Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 59% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 54% Analysis Date = 01/17/16 SpikeMix = ERA 0406-15-09: 80 µl & ERA 0406-15-07A: 80 µl Pct Recovery = 66% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 80 µl & Abs 051315: 80 µl Pct Recovery = 30% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 80 µl & ERA 0406-15-08: 80 µl Pct Recovery = 72% Analysis Date = 11/04/15 SpikeMix = Abs 052215: 80 µl & Abs 050115: 80 µl Pct Recovery = 72% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 54% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 55% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 62% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 64% Analysis Date = 11/18/16 SpikeMix = ERA 04281604: 80 µl & ERA 04281603: 80 µl Pct Recovery = 54% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & ERA 04281604: 80 µl Pct Recovery = 53% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 50% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 51% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-04: 15 µl & Abs 041814: 15 µl Pct Recovery = 86% Analysis Date = 12/06/14 SpikeMix = ERA 0318-14-02: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 77% Analysis Date = 10/25/14 SpikeMix = Abs 041614: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 84% Analysis Date = 10/11/14 SpikeMix = ERA 0318-14-02: 60 µl & ERA 0319-14-04: 60 µl Pct Recovery = 71% Analysis Date = 08/28/14 SpikeMix = ERA 0319-14-04: 60 µl & ERA 0319-14-05: 60 µl Pct Recovery = 68% Analysis Date = 05/07/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 107% Analysis Date = 03/11/15 SpikeMix = ERA 0318-14-02: 15 µl & Abs 041714: 15 µl Pct Recovery = 92% Analysis Date = 01/16/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 94% Analysis Date = 12/06/14 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 78% Analysis Date = 08/21/14 SpikeMix = ERA 0318-14-02: 60 µl & Abs 041714: 60 µl Pct Recovery = 70% Analysis Date = 07/12/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 76% Analysis Date = 06/11/14 SpikeMix = Abs 041614: 60 µl & Abs 041714: 60 µl Pct Recovery = 92% Analysis Date = 05/21/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 85% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-07A: 40 µl & Abs 051315: 40 µl Pct Recovery = 59% Analysis Date = 11/04/15 SpikeMix = ERA 0406-15-07A: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 60% Analysis Date = 09/10/15 SpikeMix = Abs 052215: 40 µl & ERA 0406-15-07A: 40 µl Pct Recovery = 70% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 72% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 62% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 66% Analysis Date = 02/23/16 SpikeMix = Abs 052215: 40 µl & Abs 050115: 40 µl Pct Recovery = 73% Analysis Date = 07/31/15 SpikeMix = ERA 0406-15-09: 40 µl & Abs 050115: 40 µl Pct Recovery = 77% Analysis Date = 07/30/15 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 70% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 73% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 78% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 60% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 57% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 57% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 58% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 44% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 49% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 53% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 45% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 49% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 47% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 44% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 45% Analysis Date = 04/30/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 75% Analysis Date = 04/10/15 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 70% Analysis Date = 02/10/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 106% Analysis Date = 12/07/14 SpikeMix = ERA 0318-14-02: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 78% Analysis Date = 10/11/14 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 73% Analysis Date = 11/04/14 SpikeMix = Abs 041714: 8 µl & ERA 0319-14-05: 8 µl Pct Recovery = 71% Analysis Date = 09/12/14 SpikeMix = Abs 041614: 30 µl & ERA 0319-14-04: 30 µl Pct Recovery = 75% Analysis Date = 08/16/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 74% Analysis Date = 07/13/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 74% Analysis Date = 10/10/14 SpikeMix = Abs 041714: 30 µl & Abs 041814: 30 µl Pct Recovery = 76% Analysis Date = 07/20/14 SpikeMix = ERA 0318-14-02: 30 µl & Abs 041714: 30 µl Pct Recovery = 66% Analysis Date = 06/28/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 71% Analysis Date = 05/17/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 78% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 62% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 54% Analysis Date = 04/27/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 94% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 76% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 74% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 63% Analysis Date = 11/24/15 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 75% Analysis Date = 09/15/15 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 78% Analysis Date = 11/25/15 SpikeMix = Abs 050115: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 77% Analysis Date = 11/24/15 SpikeMix = ERA 0406-15-09: 20 µl & Abs 050115: 20 µl Pct Recovery = 76% Analysis Date = 08/27/15 SpikeMix = Abs 052215: 20 µl & Abs 050115: 20 µl Pct Recovery = 64% Analysis Date = 08/11/15 SpikeMix = Abs 050115: 20 µl & Abs 051315: 20 µl Pct Recovery = 54% Analysis Date = 07/09/15 SpikeMix = Abs 050115: 20 µl & Abs 052215: 20 µl Pct Recovery = 60% Analysis Date = 06/09/15 SpikeMix = Abs 051315: 20 µl & Abs 050115: 20 µl Pct Recovery = 63% Analysis Date = 01/18/17 Pct Recovery = 53% Analysis Date = 01/14/17 Pct Recovery = 53% Analysis Date = 01/14/17 Pct Recovery = 53% Analysis Date = 01/09/17 Pct Recovery = 53% Analysis Date = 01/09/17 Pct Recovery = 53% Analysis Date = 01/04/17 Pct Recovery = 53% Analysis Date = 01/04/17 Pct Recovery = 53% Analysis Date = 12/30/16 Pct Recovery = 53% Analysis Date = 12/30/16 Pct Recovery = 53% Analysis Date = 12/25/16 Pct Recovery = 54% Analysis Date = 12/25/16 Pct Recovery = 54% Analysis Date = 12/20/16 Pct Recovery = 54% Analysis Date = 12/20/16 Pct Recovery = 54% Analysis Date = 12/15/16 Pct Recovery = 54% Analysis Date = 12/15/16 Pct Recovery = 54% Analysis Date = 12/10/16 Pct Recovery = 54% Analysis Date = 12/10/16 Pct Recovery = 54% Analysis Date = 12/05/16 Pct Recovery = 54% Analysis Date = 12/05/16 Pct Recovery = 54% Analysis Date = 12/01/16 Pct Recovery = 54% Analysis Date = 12/01/16 Pct Recovery = 54% Analysis Date = 11/26/16 Pct Recovery = 55% Analysis Date = 11/26/16 Pct Recovery = 55% Analysis Date = 11/21/16 Pct Recovery = 55% Analysis Date = 11/21/16 Pct Recovery = 55% Analysis Date = 11/16/16 Pct Recovery = 55% Analysis Date = 11/16/16 Pct Recovery = 55% Analysis Date = 11/11/16 Pct Recovery = 55% Analysis Date = 11/11/16 Pct Recovery = 55% Analysis Date = 11/06/16 Pct Recovery = 55% Analysis Date = 11/06/16 Pct Recovery = 55% Analysis Date = 11/01/16 Pct Recovery = 56% Analysis Date = 11/01/16 Pct Recovery = 56% Analysis Date = 10/27/16 Pct Recovery = 56% Analysis Date = 10/27/16 Pct Recovery = 56% Analysis Date = 10/22/16 Pct Recovery = 56% Analysis Date = 10/22/16 Pct Recovery = 56% Analysis Date = 10/18/16 Pct Recovery = 56% Analysis Date = 10/18/16 Pct Recovery = 56% Analysis Date = 10/13/16 Pct Recovery = 56% Analysis Date = 10/13/16 Pct Recovery = 56% Analysis Date = 10/08/16 Pct Recovery = 57% Analysis Date = 10/08/16 Pct Recovery = 57% Analysis Date = 10/03/16 Pct Recovery = 57% Analysis Date = 10/03/16 Pct Recovery = 57% Analysis Date = 09/28/16 Pct Recovery = 57% Analysis Date = 09/28/16 Pct Recovery = 57% Analysis Date = 09/23/16 Pct Recovery = 57% Analysis Date = 09/23/16 Pct Recovery = 57% Analysis Date = 09/18/16 Pct Recovery = 57% Analysis Date = 09/18/16 Pct Recovery = 57% Analysis Date = 09/13/16 Pct Recovery = 58% Analysis Date = 09/13/16 Pct Recovery = 58% Analysis Date = 09/08/16 Pct Recovery = 58% Analysis Date = 09/08/16 Pct Recovery = 58% Analysis Date = 09/04/16 Pct Recovery = 58% Analysis Date = 09/04/16 Pct Recovery = 58% Analysis Date = 08/30/16 Pct Recovery = 58% Analysis Date = 08/30/16 Pct Recovery = 58% Analysis Date = 08/25/16 Pct Recovery = 58% Analysis Date = 08/25/16 Pct Recovery = 58% Analysis Date = 08/20/16 Pct Recovery = 59% Analysis Date = 08/20/16 Pct Recovery = 59% Analysis Date = 08/15/16 Pct Recovery = 59% Analysis Date = 08/15/16 Pct Recovery = 59% Analysis Date = 08/10/16 Pct Recovery = 59% Analysis Date = 08/10/16 Pct Recovery = 59% Analysis Date = 08/05/16 Pct Recovery = 59% Analysis Date = 08/05/16 Pct Recovery = 59% Analysis Date = 07/31/16 Pct Recovery = 59% Analysis Date = 07/31/16 Pct Recovery = 59% Analysis Date = 07/26/16 Pct Recovery = 60% Analysis Date = 07/26/16 Pct Recovery = 60% Analysis Date = 07/22/16 Pct Recovery = 60% Analysis Date = 07/22/16 Pct Recovery = 60% Analysis Date = 07/17/16 Pct Recovery = 60% Analysis Date = 07/17/16 Pct Recovery = 60% Analysis Date = 07/12/16 Pct Recovery = 60% Analysis Date = 07/12/16 Pct Recovery = 60% Analysis Date = 07/07/16 Pct Recovery = 60% Analysis Date = 07/07/16 Pct Recovery = 60% Analysis Date = 07/02/16 Pct Recovery = 61% Analysis Date = 07/02/16 Pct Recovery = 61% Analysis Date = 06/27/16 Pct Recovery = 61% Analysis Date = 06/27/16 Pct Recovery = 61% Analysis Date = 06/22/16 Pct Recovery = 61% Analysis Date = 06/22/16 Pct Recovery = 61% Analysis Date = 06/17/16 Pct Recovery = 61% Analysis Date = 06/17/16 Pct Recovery = 61% Analysis Date = 06/12/16 Pct Recovery = 62% Analysis Date = 06/12/16 Pct Recovery = 62% Analysis Date = 06/08/16 Pct Recovery = 62% Analysis Date = 06/08/16 Pct Recovery = 62% Analysis Date = 06/03/16 Pct Recovery = 62% Analysis Date = 06/03/16 Pct Recovery = 62% Analysis Date = 05/29/16 Pct Recovery = 62% Analysis Date = 05/29/16 Pct Recovery = 62% Analysis Date = 05/24/16 Pct Recovery = 62% Analysis Date = 05/24/16 Pct Recovery = 62% Analysis Date = 05/19/16 Pct Recovery = 63% Analysis Date = 05/19/16 Pct Recovery = 63% Analysis Date = 05/14/16 Pct Recovery = 63% Analysis Date = 05/14/16 Pct Recovery = 63% Analysis Date = 05/09/16 Pct Recovery = 63% Analysis Date = 05/09/16 Pct Recovery = 63% Analysis Date = 05/04/16 Pct Recovery = 63% Analysis Date = 05/04/16 Pct Recovery = 63% Analysis Date = 04/29/16 Pct Recovery = 64% Analysis Date = 04/29/16 Pct Recovery = 64% Analysis Date = 04/25/16 Pct Recovery = 64% Analysis Date = 04/25/16 Pct Recovery = 64% Analysis Date = 04/20/16 Pct Recovery = 64% Analysis Date = 04/20/16 Pct Recovery = 64% Analysis Date = 04/15/16 Pct Recovery = 64% Analysis Date = 04/15/16 Pct Recovery = 64% Analysis Date = 04/10/16 Pct Recovery = 64% Analysis Date = 04/10/16 Pct Recovery = 64% Analysis Date = 04/05/16 Pct Recovery = 64% Analysis Date = 04/05/16 Pct Recovery = 64% Analysis Date = 03/31/16 Pct Recovery = 65% Analysis Date = 03/31/16 Pct Recovery = 65% Analysis Date = 03/26/16 Pct Recovery = 65% Analysis Date = 03/26/16 Pct Recovery = 65% Analysis Date = 03/21/16 Pct Recovery = 65% Analysis Date = 03/21/16 Pct Recovery = 65% Analysis Date = 03/16/16 Pct Recovery = 65% Analysis Date = 03/16/16 Pct Recovery = 65% Analysis Date = 03/12/16 Pct Recovery = 65% Analysis Date = 03/12/16 Pct Recovery = 65% Analysis Date = 03/07/16 Pct Recovery = 66% Analysis Date = 03/07/16 Pct Recovery = 66% Analysis Date = 03/02/16 Pct Recovery = 66% Analysis Date = 03/02/16 Pct Recovery = 66% Analysis Date = 02/26/16 Pct Recovery = 66% Analysis Date = 02/26/16 Pct Recovery = 66% Analysis Date = 02/21/16 Pct Recovery = 66% Analysis Date = 02/21/16 Pct Recovery = 66% Analysis Date = 02/16/16 Pct Recovery = 66% Analysis Date = 02/16/16 Pct Recovery = 66% Analysis Date = 02/11/16 Pct Recovery = 66% Analysis Date = 02/11/16 Pct Recovery = 66% Analysis Date = 02/06/16 Pct Recovery = 66% Analysis Date = 02/06/16 Pct Recovery = 66% Analysis Date = 02/01/16 Pct Recovery = 67% Analysis Date = 02/01/16 Pct Recovery = 67% Analysis Date = 01/28/16 Pct Recovery = 67% Analysis Date = 01/28/16 Pct Recovery = 67% Analysis Date = 01/23/16 Pct Recovery = 67% Analysis Date = 01/23/16 Pct Recovery = 67% Analysis Date = 01/18/16 Pct Recovery = 67% Analysis Date = 01/18/16 Pct Recovery = 67% Analysis Date = 01/13/16 Pct Recovery = 67% Analysis Date = 01/13/16 Pct Recovery = 67% Analysis Date = 01/08/16 Pct Recovery = 67% Analysis Date = 01/08/16 Pct Recovery = 67% Analysis Date = 01/03/16 Pct Recovery = 67% Analysis Date = 01/03/16 Pct Recovery = 67% Analysis Date = 12/29/15 Pct Recovery = 67% Analysis Date = 12/29/15 Pct Recovery = 67% Analysis Date = 12/24/15 Pct Recovery = 67% Analysis Date = 12/24/15 Pct Recovery = 67% Analysis Date = 12/19/15 Pct Recovery = 67% Analysis Date = 12/19/15 Pct Recovery = 67% Analysis Date = 12/15/15 Pct Recovery = 68% Analysis Date = 12/15/15 Pct Recovery = 68% Analysis Date = 12/10/15 Pct Recovery = 68% Analysis Date = 12/10/15 Pct Recovery = 68% Analysis Date = 12/05/15 Pct Recovery = 68% Analysis Date = 12/05/15 Pct Recovery = 68% Analysis Date = 11/30/15 Pct Recovery = 68% Analysis Date = 11/30/15 Pct Recovery = 68% Analysis Date = 11/25/15 Pct Recovery = 68% Analysis Date = 11/25/15 Pct Recovery = 68% Analysis Date = 11/20/15 Pct Recovery = 68% Analysis Date = 11/20/15 Pct Recovery = 68% Analysis Date = 11/15/15 Pct Recovery = 68% Analysis Date = 11/15/15 Pct Recovery = 68% Analysis Date = 11/10/15 Pct Recovery = 69% Analysis Date = 11/10/15 Pct Recovery = 69% Analysis Date = 11/05/15 Pct Recovery = 69% Analysis Date = 11/05/15 Pct Recovery = 69% Analysis Date = 11/01/15 Pct Recovery = 69% Analysis Date = 11/01/15 Pct Recovery = 69% Analysis Date = 10/27/15 Pct Recovery = 69% Analysis Date = 10/27/15 Pct Recovery = 69% Analysis Date = 10/22/15 Pct Recovery = 69% Analysis Date = 10/22/15 Pct Recovery = 69% Analysis Date = 10/17/15 Pct Recovery = 70% Analysis Date = 10/17/15 Pct Recovery = 70% Analysis Date = 10/12/15 Pct Recovery = 70% Analysis Date = 10/12/15 Pct Recovery = 70% Analysis Date = 10/07/15 Pct Recovery = 70% Analysis Date = 10/07/15 Pct Recovery = 70% Analysis Date = 10/02/15 Pct Recovery = 70% Analysis Date = 10/02/15 Pct Recovery = 70% Analysis Date = 09/27/15 Pct Recovery = 70% Analysis Date = 09/27/15 Pct Recovery = 70% Analysis Date = 09/22/15 Pct Recovery = 71% Analysis Date = 09/22/15 Pct Recovery = 71% Analysis Date = 09/17/15 Pct Recovery = 71% Analysis Date = 09/17/15 Pct Recovery = 71% Analysis Date = 09/13/15 Pct Recovery = 71% Analysis Date = 09/13/15 Pct Recovery = 71% Analysis Date = 09/08/15 Pct Recovery = 71% Analysis Date = 09/08/15 Pct Recovery = 71% Analysis Date = 09/03/15 Pct Recovery = 71% Analysis Date = 09/03/15 Pct Recovery = 71% Analysis Date = 08/29/15 Pct Recovery = 72% Analysis Date = 08/29/15 Pct Recovery = 72% Analysis Date = 08/24/15 Pct Recovery = 72% Analysis Date = 08/24/15 Pct Recovery = 72% Analysis Date = 08/19/15 Pct Recovery = 72% Analysis Date = 08/19/15 Pct Recovery = 72% Analysis Date = 08/14/15 Pct Recovery = 72% Analysis Date = 08/14/15 Pct Recovery = 72% Analysis Date = 08/09/15 Pct Recovery = 72% Analysis Date = 08/09/15 Pct Recovery = 72% Analysis Date = 08/04/15 Pct Recovery = 73% Analysis Date = 08/04/15 Pct Recovery = 73% Analysis Date = 07/31/15 Pct Recovery = 73% Analysis Date = 07/31/15 Pct Recovery = 73% Analysis Date = 07/26/15 Pct Recovery = 73% Analysis Date = 07/26/15 Pct Recovery = 73% Analysis Date = 07/21/15 Pct Recovery = 73% Analysis Date = 07/21/15 Pct Recovery = 73% Analysis Date = 07/16/15 Pct Recovery = 73% Analysis Date = 07/16/15 Pct Recovery = 73% Analysis Date = 07/11/15 Pct Recovery = 73% Analysis Date = 07/11/15 Pct Recovery = 73% Analysis Date = 07/06/15 Pct Recovery = 73% Analysis Date = 07/06/15 Pct Recovery = 73% Analysis Date = 07/01/15 Pct Recovery = 74% Analysis Date = 07/01/15 Pct Recovery = 74% Analysis Date = 06/26/15 Pct Recovery = 74% Analysis Date = 06/26/15 Pct Recovery = 74% Analysis Date = 06/21/15 Pct Recovery = 74% Analysis Date = 06/21/15 Pct Recovery = 74% Analysis Date = 06/17/15 Pct Recovery = 74% Analysis Date = 06/17/15 Pct Recovery = 74% Analysis Date = 06/12/15 Pct Recovery = 74% Analysis Date = 06/12/15 Pct Recovery = 74% Analysis Date = 06/07/15 Pct Recovery = 74% Analysis Date = 06/07/15 Pct Recovery = 74% Analysis Date = 06/02/15 Pct Recovery = 74% Analysis Date = 06/02/15 Pct Recovery = 74% Analysis Date = 05/28/15 Pct Recovery = 74% Analysis Date = 05/28/15 Pct Recovery = 74% Analysis Date = 05/23/15 Pct Recovery = 74% Analysis Date = 05/23/15 Pct Recovery = 74% Analysis Date = 05/18/15 Pct Recovery = 74% Analysis Date = 05/18/15 Pct Recovery = 74% Analysis Date = 05/13/15 Pct Recovery = 75% Analysis Date = 05/13/15 Pct Recovery = 75% Analysis Date = 05/08/15 Pct Recovery = 75% Analysis Date = 05/08/15 Pct Recovery = 75% Analysis Date = 05/04/15 Pct Recovery = 75% Analysis Date = 05/04/15 Pct Recovery = 75% Analysis Date = 04/29/15 Pct Recovery = 75% Analysis Date = 04/29/15 Pct Recovery = 75% Analysis Date = 04/24/15 Pct Recovery = 75% Analysis Date = 04/24/15 Pct Recovery = 75% Analysis Date = 04/19/15 Pct Recovery = 75% Analysis Date = 04/19/15 Pct Recovery = 75% Analysis Date = 04/14/15 Pct Recovery = 75% Analysis Date = 04/14/15 Pct Recovery = 75% Analysis Date = 04/09/15 Pct Recovery = 75% Analysis Date = 04/09/15 Pct Recovery = 75% Analysis Date = 04/04/15 Pct Recovery = 75% Analysis Date = 04/04/15 Pct Recovery = 75% Analysis Date = 03/30/15 Pct Recovery = 75% Analysis Date = 03/30/15 Pct Recovery = 75% Analysis Date = 03/25/15 Pct Recovery = 75% Analysis Date = 03/25/15 Pct Recovery = 75% Analysis Date = 03/21/15 Pct Recovery = 75% Analysis Date = 03/21/15 Pct Recovery = 75% Analysis Date = 03/16/15 Pct Recovery = 75% Analysis Date = 03/16/15 Pct Recovery = 75% Analysis Date = 03/11/15 Pct Recovery = 76% Analysis Date = 03/11/15 Pct Recovery = 76% Analysis Date = 03/06/15 Pct Recovery = 76% Analysis Date = 03/06/15 Pct Recovery = 76% Analysis Date = 03/01/15 Pct Recovery = 76% Analysis Date = 03/01/15 Pct Recovery = 76% Analysis Date = 02/24/15 Pct Recovery = 76% Analysis Date = 02/24/15 Pct Recovery = 76% Analysis Date = 02/19/15 Pct Recovery = 76% Analysis Date = 02/19/15 Pct Recovery = 76% Analysis Date = 02/14/15 Pct Recovery = 76% Analysis Date = 02/14/15 Pct Recovery = 76% Analysis Date = 02/09/15 Pct Recovery = 76% Analysis Date = 02/09/15 Pct Recovery = 76% Analysis Date = 02/05/15 Pct Recovery = 76% Analysis Date = 02/05/15 Pct Recovery = 76% Analysis Date = 01/31/15 Pct Recovery = 76% Analysis Date = 01/31/15 Pct Recovery = 76% Analysis Date = 01/26/15 Pct Recovery = 76% Analysis Date = 01/26/15 Pct Recovery = 76% Analysis Date = 01/21/15 Pct Recovery = 76% Analysis Date = 01/21/15 Pct Recovery = 76% Analysis Date = 01/16/15 Pct Recovery = 76% Analysis Date = 01/16/15 Pct Recovery = 76% Analysis Date = 01/11/15 Pct Recovery = 76% Analysis Date = 01/11/15 Pct Recovery = 76% Analysis Date = 01/06/15 Pct Recovery = 76% Analysis Date = 01/06/15 Pct Recovery = 76% Analysis Date = 01/01/15 Pct Recovery = 76% Analysis Date = 01/01/15 Pct Recovery = 76% Analysis Date = 12/27/14 Pct Recovery = 77% Analysis Date = 12/27/14 Pct Recovery = 77% Analysis Date = 12/23/14 Pct Recovery = 77% Analysis Date = 12/23/14 Pct Recovery = 77% Analysis Date = 12/18/14 Pct Recovery = 77% Analysis Date = 12/18/14 Pct Recovery = 77% Analysis Date = 12/13/14 Pct Recovery = 77% Analysis Date = 12/13/14 Pct Recovery = 77% Analysis Date = 12/08/14 Pct Recovery = 77% Analysis Date = 12/08/14 Pct Recovery = 77% Analysis Date = 12/03/14 Pct Recovery = 77% Analysis Date = 12/03/14 Pct Recovery = 77% Analysis Date = 11/28/14 Pct Recovery = 77% Analysis Date = 11/28/14 Pct Recovery = 77% Analysis Date = 11/23/14 Pct Recovery = 77% Analysis Date = 11/23/14 Pct Recovery = 77% Analysis Date = 11/18/14 Pct Recovery = 77% Analysis Date = 11/18/14 Pct Recovery = 77% Analysis Date = 11/13/14 Pct Recovery = 77% Analysis Date = 11/13/14 Pct Recovery = 77% Analysis Date = 11/09/14 Pct Recovery = 77% Analysis Date = 11/09/14 Pct Recovery = 77% Analysis Date = 11/04/14 Pct Recovery = 77% Analysis Date = 11/04/14 Pct Recovery = 77% Analysis Date = 10/30/14 Pct Recovery = 77% Analysis Date = 10/30/14 Pct Recovery = 77% Analysis Date = 10/25/14 Pct Recovery = 77% Analysis Date = 10/25/14 Pct Recovery = 77% Analysis Date = 10/20/14 Pct Recovery = 77% Analysis Date = 10/20/14 Pct Recovery = 77% Analysis Date = 10/15/14 Pct Recovery = 78% Analysis Date = 10/15/14 Pct Recovery = 78% Analysis Date = 10/10/14 Pct Recovery = 78% Analysis Date = 10/10/14 Pct Recovery = 78% Analysis Date = 10/05/14 Pct Recovery = 78% Analysis Date = 10/05/14 Pct Recovery = 78% Analysis Date = 09/30/14 Pct Recovery = 78% Analysis Date = 09/30/14 Pct Recovery = 78% Analysis Date = 09/26/14 Pct Recovery = 78% Analysis Date = 09/26/14 Pct Recovery = 78% Analysis Date = 09/21/14 Pct Recovery = 78% Analysis Date = 09/21/14 Pct Recovery = 78% Analysis Date = 09/16/14 Pct Recovery = 78% Analysis Date = 09/16/14 Pct Recovery = 78% Analysis Date = 09/11/14 Pct Recovery = 78% Analysis Date = 09/11/14 Pct Recovery = 78% Analysis Date = 09/06/14 Pct Recovery = 78% Analysis Date = 09/06/14 Pct Recovery = 78% Analysis Date = 09/01/14 Pct Recovery = 78% Analysis Date = 09/01/14 Pct Recovery = 78% Analysis Date = 08/27/14 Pct Recovery = 78% Analysis Date = 08/27/14 Pct Recovery = 78% Analysis Date = 08/22/14 Pct Recovery = 78% Analysis Date = 08/22/14 Pct Recovery = 78% Analysis Date = 08/17/14 Pct Recovery = 78% Analysis Date = 08/17/14 Pct Recovery = 78% Analysis Date = 08/13/14 Pct Recovery = 78% Analysis Date = 08/13/14 Pct Recovery = 78% Analysis Date = 08/08/14 Pct Recovery = 78% Analysis Date = 08/08/14 Pct Recovery = 78% Analysis Date = 08/03/14 Pct Recovery = 78% Analysis Date = 08/03/14 Pct Recovery = 78% Analysis Date = 07/29/14 Pct Recovery = 78% Analysis Date = 07/29/14 Pct Recovery = 78% Analysis Date = 07/24/14 Pct Recovery = 78% Analysis Date = 07/24/14 Pct Recovery = 78% Analysis Date = 07/19/14 Pct Recovery = 78% Analysis Date = 07/19/14 Pct Recovery = 78% Analysis Date = 07/14/14 Pct Recovery = 78% Analysis Date = 07/14/14 Pct Recovery = 78% Analysis Date = 07/09/14 Pct Recovery = 78% Analysis Date = 07/09/14 Pct Recovery = 78% Analysis Date = 07/04/14 Pct Recovery = 78% Analysis Date = 07/04/14 Pct Recovery = 78% Analysis Date = 06/30/14 Pct Recovery = 78% Analysis Date = 06/30/14 Pct Recovery = 78% Analysis Date = 06/25/14 Pct Recovery = 78% Analysis Date = 06/25/14 Pct Recovery = 78% Analysis Date = 06/20/14 Pct Recovery = 78% Analysis Date = 06/20/14 Pct Recovery = 78% Analysis Date = 06/15/14 Pct Recovery = 78% Analysis Date = 06/15/14 Pct Recovery = 78% Analysis Date = 06/10/14 Pct Recovery = 78% Analysis Date = 06/10/14 Pct Recovery = 78% Analysis Date = 06/05/14 Pct Recovery = 78% Analysis Date = 06/05/14 Pct Recovery = 78% Analysis Date = 05/31/14 Pct Recovery = 78% Analysis Date = 05/31/14 Pct Recovery = 78% Analysis Date = 05/26/14 Pct Recovery = 78% Analysis Date = 05/26/14 Pct Recovery = 78% Analysis Date = 05/21/14 Pct Recovery = 78% Analysis Date = 05/21/14 Pct Recovery = 78% Analysis Date = 05/17/14 Pct Recovery = 78% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
DEHYDRONIFEDIPINE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 77 68% 14% 70% 14%
Total 77 68% 14% 70% 14%

Sample Statistics
DEHYDRONIFEDIPINE

Characteristic N % % Basis
Plotted 77 99% Spiked
Estimated Values 21 27% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 78 .  
False Negatives 1 1% 1 out of 78
Not Spiked 37 .  
False Positives 0 0% 0 out of 37

BQS OBSP Determination:
DESMETHYLDILTIAZEM
METHOD: 2440 , TESTIDCODE: 67999LCM56
Open Data Set

Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 20% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 26% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 80 µl & ERA 0406-15-08: 80 µl Pct Recovery = 27% Analysis Date = 01/17/16 SpikeMix = ERA 0406-15-09: 80 µl & ERA 0406-15-07A: 80 µl Pct Recovery = 52% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 80 µl & Abs 051315: 80 µl Pct Recovery = 52% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 35% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 42% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 66% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 54% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 36% Analysis Date = 12/07/14 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 46% Analysis Date = 10/25/14 SpikeMix = Abs 041614: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 50% Analysis Date = 06/22/14 SpikeMix = Abs 041814: 60 µl & Abs 041614: 60 µl Pct Recovery = 69% Analysis Date = 06/11/14 SpikeMix = Abs 041614: 60 µl & Abs 041714: 60 µl Pct Recovery = 30% Analysis Date = 04/29/15 SpikeMix = ERA 0319-14-05: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 40% Analysis Date = 03/11/15 SpikeMix = ERA 0318-14-02: 15 µl & Abs 041714: 15 µl Pct Recovery = 55% Analysis Date = 02/06/15 SpikeMix = Abs 041814: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 49% Analysis Date = 12/06/14 SpikeMix = ERA 0318-14-02: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 35% Analysis Date = 10/11/14 SpikeMix = ERA 0318-14-02: 60 µl & ERA 0319-14-04: 60 µl Pct Recovery = 36% Analysis Date = 07/26/14 SpikeMix = ERA 0319-14-05: 60 µl & ERA 0318-14-02: 60 µl Pct Recovery = 42% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 41% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 31% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-07A: 40 µl & Abs 051315: 40 µl Pct Recovery = 37% Analysis Date = 11/04/15 SpikeMix = ERA 0406-15-07A: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 42% Analysis Date = 09/10/15 SpikeMix = Abs 052215: 40 µl & ERA 0406-15-07A: 40 µl Pct Recovery = 47% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 38% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 49% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 50% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 50% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 33% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 42% Analysis Date = 04/30/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 22% Analysis Date = 02/10/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 29% Analysis Date = 10/24/14 SpikeMix = ERA 0319-14-05: 8 µl & Abs 041614: 8 µl Pct Recovery = 9% Analysis Date = 12/07/14 SpikeMix = ERA 0318-14-02: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 62% Analysis Date = 11/04/14 SpikeMix = Abs 041814: 8 µl & ERA 0318-14-02: 8 µl Pct Recovery = 38% Analysis Date = 07/13/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 46% Analysis Date = 06/28/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 23% Analysis Date = 05/30/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 37% Analysis Date = 05/17/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 52% Analysis Date = 08/30/14 SpikeMix = ERA 0318-14-02: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 37% Analysis Date = 07/20/14 SpikeMix = ERA 0318-14-02: 30 µl & Abs 041714: 30 µl Pct Recovery = 21% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 35% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 31% Analysis Date = 04/27/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 62% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 50% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 38% Analysis Date = 11/24/15 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 49% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-09: 20 µl Pct Recovery = 3% Analysis Date = 11/18/16 SpikeMix = ERA 04281604: 80 µl & ERA 04281603: 80 µl Pct Recovery = 39% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & ERA 04281604: 80 µl Pct Recovery = 33% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 47% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 49% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 63% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 56% Analysis Date = 01/18/17 Pct Recovery = 40% Analysis Date = 01/14/17 Pct Recovery = 40% Analysis Date = 01/14/17 Pct Recovery = 40% Analysis Date = 01/09/17 Pct Recovery = 41% Analysis Date = 01/09/17 Pct Recovery = 41% Analysis Date = 01/04/17 Pct Recovery = 41% Analysis Date = 01/04/17 Pct Recovery = 41% Analysis Date = 12/30/16 Pct Recovery = 41% Analysis Date = 12/30/16 Pct Recovery = 41% Analysis Date = 12/25/16 Pct Recovery = 41% Analysis Date = 12/25/16 Pct Recovery = 41% Analysis Date = 12/20/16 Pct Recovery = 41% Analysis Date = 12/20/16 Pct Recovery = 41% Analysis Date = 12/15/16 Pct Recovery = 41% Analysis Date = 12/15/16 Pct Recovery = 41% Analysis Date = 12/10/16 Pct Recovery = 41% Analysis Date = 12/10/16 Pct Recovery = 41% Analysis Date = 12/05/16 Pct Recovery = 41% Analysis Date = 12/05/16 Pct Recovery = 41% Analysis Date = 12/01/16 Pct Recovery = 41% Analysis Date = 12/01/16 Pct Recovery = 41% Analysis Date = 11/26/16 Pct Recovery = 42% Analysis Date = 11/26/16 Pct Recovery = 42% Analysis Date = 11/21/16 Pct Recovery = 42% Analysis Date = 11/21/16 Pct Recovery = 42% Analysis Date = 11/16/16 Pct Recovery = 42% Analysis Date = 11/16/16 Pct Recovery = 42% Analysis Date = 11/11/16 Pct Recovery = 42% Analysis Date = 11/11/16 Pct Recovery = 42% Analysis Date = 11/06/16 Pct Recovery = 42% Analysis Date = 11/06/16 Pct Recovery = 42% Analysis Date = 11/01/16 Pct Recovery = 42% Analysis Date = 11/01/16 Pct Recovery = 42% Analysis Date = 10/27/16 Pct Recovery = 42% Analysis Date = 10/27/16 Pct Recovery = 42% Analysis Date = 10/22/16 Pct Recovery = 42% Analysis Date = 10/22/16 Pct Recovery = 42% Analysis Date = 10/18/16 Pct Recovery = 42% Analysis Date = 10/18/16 Pct Recovery = 42% Analysis Date = 10/13/16 Pct Recovery = 42% Analysis Date = 10/13/16 Pct Recovery = 42% Analysis Date = 10/08/16 Pct Recovery = 43% Analysis Date = 10/08/16 Pct Recovery = 43% Analysis Date = 10/03/16 Pct Recovery = 43% Analysis Date = 10/03/16 Pct Recovery = 43% Analysis Date = 09/28/16 Pct Recovery = 43% Analysis Date = 09/28/16 Pct Recovery = 43% Analysis Date = 09/23/16 Pct Recovery = 43% Analysis Date = 09/23/16 Pct Recovery = 43% Analysis Date = 09/18/16 Pct Recovery = 43% Analysis Date = 09/18/16 Pct Recovery = 43% Analysis Date = 09/13/16 Pct Recovery = 43% Analysis Date = 09/13/16 Pct Recovery = 43% Analysis Date = 09/08/16 Pct Recovery = 43% Analysis Date = 09/08/16 Pct Recovery = 43% Analysis Date = 09/04/16 Pct Recovery = 43% Analysis Date = 09/04/16 Pct Recovery = 43% Analysis Date = 08/30/16 Pct Recovery = 43% Analysis Date = 08/30/16 Pct Recovery = 43% Analysis Date = 08/25/16 Pct Recovery = 43% Analysis Date = 08/25/16 Pct Recovery = 43% Analysis Date = 08/20/16 Pct Recovery = 43% Analysis Date = 08/20/16 Pct Recovery = 43% Analysis Date = 08/15/16 Pct Recovery = 43% Analysis Date = 08/15/16 Pct Recovery = 43% Analysis Date = 08/10/16 Pct Recovery = 43% Analysis Date = 08/10/16 Pct Recovery = 43% Analysis Date = 08/05/16 Pct Recovery = 43% Analysis Date = 08/05/16 Pct Recovery = 43% Analysis Date = 07/31/16 Pct Recovery = 43% Analysis Date = 07/31/16 Pct Recovery = 43% Analysis Date = 07/26/16 Pct Recovery = 44% Analysis Date = 07/26/16 Pct Recovery = 44% Analysis Date = 07/22/16 Pct Recovery = 44% Analysis Date = 07/22/16 Pct Recovery = 44% Analysis Date = 07/17/16 Pct Recovery = 44% Analysis Date = 07/17/16 Pct Recovery = 44% Analysis Date = 07/12/16 Pct Recovery = 43% Analysis Date = 07/12/16 Pct Recovery = 43% Analysis Date = 07/07/16 Pct Recovery = 43% Analysis Date = 07/07/16 Pct Recovery = 43% Analysis Date = 07/02/16 Pct Recovery = 43% Analysis Date = 07/02/16 Pct Recovery = 43% Analysis Date = 06/27/16 Pct Recovery = 43% Analysis Date = 06/27/16 Pct Recovery = 43% Analysis Date = 06/22/16 Pct Recovery = 43% Analysis Date = 06/22/16 Pct Recovery = 43% Analysis Date = 06/17/16 Pct Recovery = 43% Analysis Date = 06/17/16 Pct Recovery = 43% Analysis Date = 06/12/16 Pct Recovery = 43% Analysis Date = 06/12/16 Pct Recovery = 43% Analysis Date = 06/08/16 Pct Recovery = 43% Analysis Date = 06/08/16 Pct Recovery = 43% Analysis Date = 06/03/16 Pct Recovery = 43% Analysis Date = 06/03/16 Pct Recovery = 43% Analysis Date = 05/29/16 Pct Recovery = 43% Analysis Date = 05/29/16 Pct Recovery = 43% Analysis Date = 05/24/16 Pct Recovery = 43% Analysis Date = 05/24/16 Pct Recovery = 43% Analysis Date = 05/19/16 Pct Recovery = 43% Analysis Date = 05/19/16 Pct Recovery = 43% Analysis Date = 05/14/16 Pct Recovery = 43% Analysis Date = 05/14/16 Pct Recovery = 43% Analysis Date = 05/09/16 Pct Recovery = 43% Analysis Date = 05/09/16 Pct Recovery = 43% Analysis Date = 05/04/16 Pct Recovery = 43% Analysis Date = 05/04/16 Pct Recovery = 43% Analysis Date = 04/29/16 Pct Recovery = 43% Analysis Date = 04/29/16 Pct Recovery = 43% Analysis Date = 04/25/16 Pct Recovery = 43% Analysis Date = 04/25/16 Pct Recovery = 43% Analysis Date = 04/20/16 Pct Recovery = 43% Analysis Date = 04/20/16 Pct Recovery = 43% Analysis Date = 04/15/16 Pct Recovery = 42% Analysis Date = 04/15/16 Pct Recovery = 42% Analysis Date = 04/10/16 Pct Recovery = 42% Analysis Date = 04/10/16 Pct Recovery = 42% Analysis Date = 04/05/16 Pct Recovery = 42% Analysis Date = 04/05/16 Pct Recovery = 42% Analysis Date = 03/31/16 Pct Recovery = 42% Analysis Date = 03/31/16 Pct Recovery = 42% Analysis Date = 03/26/16 Pct Recovery = 42% Analysis Date = 03/26/16 Pct Recovery = 42% Analysis Date = 03/21/16 Pct Recovery = 42% Analysis Date = 03/21/16 Pct Recovery = 42% Analysis Date = 03/16/16 Pct Recovery = 42% Analysis Date = 03/16/16 Pct Recovery = 42% Analysis Date = 03/12/16 Pct Recovery = 42% Analysis Date = 03/12/16 Pct Recovery = 42% Analysis Date = 03/07/16 Pct Recovery = 41% Analysis Date = 03/07/16 Pct Recovery = 41% Analysis Date = 03/02/16 Pct Recovery = 41% Analysis Date = 03/02/16 Pct Recovery = 41% Analysis Date = 02/26/16 Pct Recovery = 41% Analysis Date = 02/26/16 Pct Recovery = 41% Analysis Date = 02/21/16 Pct Recovery = 41% Analysis Date = 02/21/16 Pct Recovery = 41% Analysis Date = 02/16/16 Pct Recovery = 41% Analysis Date = 02/16/16 Pct Recovery = 41% Analysis Date = 02/11/16 Pct Recovery = 41% Analysis Date = 02/11/16 Pct Recovery = 41% Analysis Date = 02/06/16 Pct Recovery = 41% Analysis Date = 02/06/16 Pct Recovery = 41% Analysis Date = 02/01/16 Pct Recovery = 41% Analysis Date = 02/01/16 Pct Recovery = 41% Analysis Date = 01/28/16 Pct Recovery = 40% Analysis Date = 01/28/16 Pct Recovery = 40% Analysis Date = 01/23/16 Pct Recovery = 40% Analysis Date = 01/23/16 Pct Recovery = 40% Analysis Date = 01/18/16 Pct Recovery = 40% Analysis Date = 01/18/16 Pct Recovery = 40% Analysis Date = 01/13/16 Pct Recovery = 40% Analysis Date = 01/13/16 Pct Recovery = 40% Analysis Date = 01/08/16 Pct Recovery = 40% Analysis Date = 01/08/16 Pct Recovery = 40% Analysis Date = 01/03/16 Pct Recovery = 40% Analysis Date = 01/03/16 Pct Recovery = 40% Analysis Date = 12/29/15 Pct Recovery = 40% Analysis Date = 12/29/15 Pct Recovery = 40% Analysis Date = 12/24/15 Pct Recovery = 40% Analysis Date = 12/24/15 Pct Recovery = 40% Analysis Date = 12/19/15 Pct Recovery = 39% Analysis Date = 12/19/15 Pct Recovery = 39% Analysis Date = 12/15/15 Pct Recovery = 39% Analysis Date = 12/15/15 Pct Recovery = 39% Analysis Date = 12/10/15 Pct Recovery = 39% Analysis Date = 12/10/15 Pct Recovery = 39% Analysis Date = 12/05/15 Pct Recovery = 39% Analysis Date = 12/05/15 Pct Recovery = 39% Analysis Date = 11/30/15 Pct Recovery = 39% Analysis Date = 11/30/15 Pct Recovery = 39% Analysis Date = 11/25/15 Pct Recovery = 39% Analysis Date = 11/25/15 Pct Recovery = 39% Analysis Date = 11/20/15 Pct Recovery = 39% Analysis Date = 11/20/15 Pct Recovery = 39% Analysis Date = 11/15/15 Pct Recovery = 39% Analysis Date = 11/15/15 Pct Recovery = 39% Analysis Date = 11/10/15 Pct Recovery = 39% Analysis Date = 11/10/15 Pct Recovery = 39% Analysis Date = 11/05/15 Pct Recovery = 39% Analysis Date = 11/05/15 Pct Recovery = 39% Analysis Date = 11/01/15 Pct Recovery = 39% Analysis Date = 11/01/15 Pct Recovery = 39% Analysis Date = 10/27/15 Pct Recovery = 39% Analysis Date = 10/27/15 Pct Recovery = 39% Analysis Date = 10/22/15 Pct Recovery = 39% Analysis Date = 10/22/15 Pct Recovery = 39% Analysis Date = 10/17/15 Pct Recovery = 39% Analysis Date = 10/17/15 Pct Recovery = 39% Analysis Date = 10/12/15 Pct Recovery = 39% Analysis Date = 10/12/15 Pct Recovery = 39% Analysis Date = 10/07/15 Pct Recovery = 39% Analysis Date = 10/07/15 Pct Recovery = 39% Analysis Date = 10/02/15 Pct Recovery = 39% Analysis Date = 10/02/15 Pct Recovery = 39% Analysis Date = 09/27/15 Pct Recovery = 39% Analysis Date = 09/27/15 Pct Recovery = 39% Analysis Date = 09/22/15 Pct Recovery = 39% Analysis Date = 09/22/15 Pct Recovery = 39% Analysis Date = 09/17/15 Pct Recovery = 39% Analysis Date = 09/17/15 Pct Recovery = 39% Analysis Date = 09/13/15 Pct Recovery = 39% Analysis Date = 09/13/15 Pct Recovery = 39% Analysis Date = 09/08/15 Pct Recovery = 39% Analysis Date = 09/08/15 Pct Recovery = 39% Analysis Date = 09/03/15 Pct Recovery = 39% Analysis Date = 09/03/15 Pct Recovery = 39% Analysis Date = 08/29/15 Pct Recovery = 39% Analysis Date = 08/29/15 Pct Recovery = 39% Analysis Date = 08/24/15 Pct Recovery = 39% Analysis Date = 08/24/15 Pct Recovery = 39% Analysis Date = 08/19/15 Pct Recovery = 39% Analysis Date = 08/19/15 Pct Recovery = 39% Analysis Date = 08/14/15 Pct Recovery = 39% Analysis Date = 08/14/15 Pct Recovery = 39% Analysis Date = 08/09/15 Pct Recovery = 39% Analysis Date = 08/09/15 Pct Recovery = 39% Analysis Date = 08/04/15 Pct Recovery = 39% Analysis Date = 08/04/15 Pct Recovery = 39% Analysis Date = 07/31/15 Pct Recovery = 39% Analysis Date = 07/31/15 Pct Recovery = 39% Analysis Date = 07/26/15 Pct Recovery = 39% Analysis Date = 07/26/15 Pct Recovery = 39% Analysis Date = 07/21/15 Pct Recovery = 39% Analysis Date = 07/21/15 Pct Recovery = 39% Analysis Date = 07/16/15 Pct Recovery = 39% Analysis Date = 07/16/15 Pct Recovery = 39% Analysis Date = 07/11/15 Pct Recovery = 39% Analysis Date = 07/11/15 Pct Recovery = 39% Analysis Date = 07/06/15 Pct Recovery = 39% Analysis Date = 07/06/15 Pct Recovery = 39% Analysis Date = 07/01/15 Pct Recovery = 39% Analysis Date = 07/01/15 Pct Recovery = 39% Analysis Date = 06/26/15 Pct Recovery = 39% Analysis Date = 06/26/15 Pct Recovery = 39% Analysis Date = 06/21/15 Pct Recovery = 39% Analysis Date = 06/21/15 Pct Recovery = 39% Analysis Date = 06/17/15 Pct Recovery = 39% Analysis Date = 06/17/15 Pct Recovery = 39% Analysis Date = 06/12/15 Pct Recovery = 39% Analysis Date = 06/12/15 Pct Recovery = 39% Analysis Date = 06/07/15 Pct Recovery = 39% Analysis Date = 06/07/15 Pct Recovery = 39% Analysis Date = 06/02/15 Pct Recovery = 39% Analysis Date = 06/02/15 Pct Recovery = 39% Analysis Date = 05/28/15 Pct Recovery = 39% Analysis Date = 05/28/15 Pct Recovery = 39% Analysis Date = 05/23/15 Pct Recovery = 39% Analysis Date = 05/23/15 Pct Recovery = 39% Analysis Date = 05/18/15 Pct Recovery = 39% Analysis Date = 05/18/15 Pct Recovery = 39% Analysis Date = 05/13/15 Pct Recovery = 39% Analysis Date = 05/13/15 Pct Recovery = 39% Analysis Date = 05/08/15 Pct Recovery = 39% Analysis Date = 05/08/15 Pct Recovery = 39% Analysis Date = 05/04/15 Pct Recovery = 39% Analysis Date = 05/04/15 Pct Recovery = 39% Analysis Date = 04/29/15 Pct Recovery = 39% Analysis Date = 04/29/15 Pct Recovery = 39% Analysis Date = 04/24/15 Pct Recovery = 39% Analysis Date = 04/24/15 Pct Recovery = 39% Analysis Date = 04/19/15 Pct Recovery = 39% Analysis Date = 04/19/15 Pct Recovery = 39% Analysis Date = 04/14/15 Pct Recovery = 39% Analysis Date = 04/14/15 Pct Recovery = 39% Analysis Date = 04/09/15 Pct Recovery = 39% Analysis Date = 04/09/15 Pct Recovery = 39% Analysis Date = 04/04/15 Pct Recovery = 39% Analysis Date = 04/04/15 Pct Recovery = 39% Analysis Date = 03/30/15 Pct Recovery = 39% Analysis Date = 03/30/15 Pct Recovery = 39% Analysis Date = 03/25/15 Pct Recovery = 39% Analysis Date = 03/25/15 Pct Recovery = 39% Analysis Date = 03/21/15 Pct Recovery = 39% Analysis Date = 03/21/15 Pct Recovery = 39% Analysis Date = 03/16/15 Pct Recovery = 39% Analysis Date = 03/16/15 Pct Recovery = 39% Analysis Date = 03/11/15 Pct Recovery = 39% Analysis Date = 03/11/15 Pct Recovery = 39% Analysis Date = 03/06/15 Pct Recovery = 39% Analysis Date = 03/06/15 Pct Recovery = 39% Analysis Date = 03/01/15 Pct Recovery = 39% Analysis Date = 03/01/15 Pct Recovery = 39% Analysis Date = 02/24/15 Pct Recovery = 39% Analysis Date = 02/24/15 Pct Recovery = 39% Analysis Date = 02/19/15 Pct Recovery = 39% Analysis Date = 02/19/15 Pct Recovery = 39% Analysis Date = 02/14/15 Pct Recovery = 39% Analysis Date = 02/14/15 Pct Recovery = 39% Analysis Date = 02/09/15 Pct Recovery = 39% Analysis Date = 02/09/15 Pct Recovery = 39% Analysis Date = 02/05/15 Pct Recovery = 39% Analysis Date = 02/05/15 Pct Recovery = 39% Analysis Date = 01/31/15 Pct Recovery = 39% Analysis Date = 01/31/15 Pct Recovery = 39% Analysis Date = 01/26/15 Pct Recovery = 39% Analysis Date = 01/26/15 Pct Recovery = 39% Analysis Date = 01/21/15 Pct Recovery = 39% Analysis Date = 01/21/15 Pct Recovery = 39% Analysis Date = 01/16/15 Pct Recovery = 39% Analysis Date = 01/16/15 Pct Recovery = 39% Analysis Date = 01/11/15 Pct Recovery = 39% Analysis Date = 01/11/15 Pct Recovery = 39% Analysis Date = 01/06/15 Pct Recovery = 39% Analysis Date = 01/06/15 Pct Recovery = 39% Analysis Date = 01/01/15 Pct Recovery = 39% Analysis Date = 01/01/15 Pct Recovery = 39% Analysis Date = 12/27/14 Pct Recovery = 39% Analysis Date = 12/27/14 Pct Recovery = 39% Analysis Date = 12/23/14 Pct Recovery = 39% Analysis Date = 12/23/14 Pct Recovery = 39% Analysis Date = 12/18/14 Pct Recovery = 39% Analysis Date = 12/18/14 Pct Recovery = 39% Analysis Date = 12/13/14 Pct Recovery = 39% Analysis Date = 12/13/14 Pct Recovery = 39% Analysis Date = 12/08/14 Pct Recovery = 39% Analysis Date = 12/08/14 Pct Recovery = 39% Analysis Date = 12/03/14 Pct Recovery = 39% Analysis Date = 12/03/14 Pct Recovery = 39% Analysis Date = 11/28/14 Pct Recovery = 39% Analysis Date = 11/28/14 Pct Recovery = 39% Analysis Date = 11/23/14 Pct Recovery = 39% Analysis Date = 11/23/14 Pct Recovery = 39% Analysis Date = 11/18/14 Pct Recovery = 39% Analysis Date = 11/18/14 Pct Recovery = 39% Analysis Date = 11/13/14 Pct Recovery = 39% Analysis Date = 11/13/14 Pct Recovery = 39% Analysis Date = 11/09/14 Pct Recovery = 39% Analysis Date = 11/09/14 Pct Recovery = 39% Analysis Date = 11/04/14 Pct Recovery = 39% Analysis Date = 11/04/14 Pct Recovery = 39% Analysis Date = 10/30/14 Pct Recovery = 39% Analysis Date = 10/30/14 Pct Recovery = 39% Analysis Date = 10/25/14 Pct Recovery = 39% Analysis Date = 10/25/14 Pct Recovery = 39% Analysis Date = 10/20/14 Pct Recovery = 39% Analysis Date = 10/20/14 Pct Recovery = 39% Analysis Date = 10/15/14 Pct Recovery = 39% Analysis Date = 10/15/14 Pct Recovery = 39% Analysis Date = 10/10/14 Pct Recovery = 39% Analysis Date = 10/10/14 Pct Recovery = 39% Analysis Date = 10/05/14 Pct Recovery = 39% Analysis Date = 10/05/14 Pct Recovery = 39% Analysis Date = 09/30/14 Pct Recovery = 39% Analysis Date = 09/30/14 Pct Recovery = 39% Analysis Date = 09/26/14 Pct Recovery = 39% Analysis Date = 09/26/14 Pct Recovery = 39% Analysis Date = 09/21/14 Pct Recovery = 39% Analysis Date = 09/21/14 Pct Recovery = 39% Analysis Date = 09/16/14 Pct Recovery = 40% Analysis Date = 09/16/14 Pct Recovery = 40% Analysis Date = 09/11/14 Pct Recovery = 40% Analysis Date = 09/11/14 Pct Recovery = 40% Analysis Date = 09/06/14 Pct Recovery = 40% Analysis Date = 09/06/14 Pct Recovery = 40% Analysis Date = 09/01/14 Pct Recovery = 40% Analysis Date = 09/01/14 Pct Recovery = 40% Analysis Date = 08/27/14 Pct Recovery = 40% Analysis Date = 08/27/14 Pct Recovery = 40% Analysis Date = 08/22/14 Pct Recovery = 40% Analysis Date = 08/22/14 Pct Recovery = 40% Analysis Date = 08/17/14 Pct Recovery = 40% Analysis Date = 08/17/14 Pct Recovery = 40% Analysis Date = 08/13/14 Pct Recovery = 40% Analysis Date = 08/13/14 Pct Recovery = 40% Analysis Date = 08/08/14 Pct Recovery = 40% Analysis Date = 08/08/14 Pct Recovery = 40% Analysis Date = 08/03/14 Pct Recovery = 40% Analysis Date = 08/03/14 Pct Recovery = 40% Analysis Date = 07/29/14 Pct Recovery = 40% Analysis Date = 07/29/14 Pct Recovery = 40% Analysis Date = 07/24/14 Pct Recovery = 40% Analysis Date = 07/24/14 Pct Recovery = 40% Analysis Date = 07/19/14 Pct Recovery = 40% Analysis Date = 07/19/14 Pct Recovery = 40% Analysis Date = 07/14/14 Pct Recovery = 40% Analysis Date = 07/14/14 Pct Recovery = 40% Analysis Date = 07/09/14 Pct Recovery = 40% Analysis Date = 07/09/14 Pct Recovery = 40% Analysis Date = 07/04/14 Pct Recovery = 40% Analysis Date = 07/04/14 Pct Recovery = 40% Analysis Date = 06/30/14 Pct Recovery = 40% Analysis Date = 06/30/14 Pct Recovery = 40% Analysis Date = 06/25/14 Pct Recovery = 40% Analysis Date = 06/25/14 Pct Recovery = 40% Analysis Date = 06/20/14 Pct Recovery = 40% Analysis Date = 06/20/14 Pct Recovery = 40% Analysis Date = 06/15/14 Pct Recovery = 40% Analysis Date = 06/15/14 Pct Recovery = 40% Analysis Date = 06/10/14 Pct Recovery = 40% Analysis Date = 06/10/14 Pct Recovery = 40% Analysis Date = 06/05/14 Pct Recovery = 40% Analysis Date = 06/05/14 Pct Recovery = 40% Analysis Date = 05/31/14 Pct Recovery = 40% Analysis Date = 05/31/14 Pct Recovery = 40% Analysis Date = 05/26/14 Pct Recovery = 40% Analysis Date = 05/26/14 Pct Recovery = 40% Analysis Date = 05/21/14 Pct Recovery = 40% Analysis Date = 05/21/14 Pct Recovery = 40% Analysis Date = 05/17/14 Pct Recovery = 40% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
DESMETHYLDILTIAZEM

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 6 48% 11% 48% 13%
>= Reporting Level 49 40% 14% 40% 12%
Total 55 41% 13% 41% 12%

Sample Statistics
DESMETHYLDILTIAZEM

Characteristic N % % Basis
Plotted 55 71% Spiked
Estimated Values 55 71% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 6 8% Spiked
Spiked 77 .  
False Negatives 16 21% 16 out of 77
Not Spiked 38 .  
False Positives 0 0% 0 out of 38

BQS OBSP Determination:
DESVENLAFAXINE
METHOD: 2440 , TESTIDCODE: 68251LCM56
Open Data Set

Analysis Date = 02/23/16 SpikeMix = Abs 050115: 80 µl & ERA 0406-15-08: 80 µl Pct Recovery = 80% Analysis Date = 11/05/15 SpikeMix = ERA 0406-15-08: 80 µl & Abs 052215: 80 µl Pct Recovery = 86% Analysis Date = 11/24/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 90% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 80 µl & Abs 051315: 80 µl Pct Recovery = 86% Analysis Date = 10/01/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 66% Analysis Date = 09/24/16 SpikeMix = Crescent EN160610015: 80 µl & Abs 061416: 80 µl Pct Recovery = 75% Analysis Date = 09/24/16 SpikeMix = Abs 061416: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 71% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 90% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 90% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 88% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 81% Analysis Date = 05/07/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 65% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-04: 15 µl & Abs 041814: 15 µl Pct Recovery = 75% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 89% Analysis Date = 02/06/15 SpikeMix = Abs 041814: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 84% Analysis Date = 01/16/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 94% Analysis Date = 12/07/14 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 81% Analysis Date = 12/06/14 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 69% Analysis Date = 08/28/14 SpikeMix = ERA 0319-14-04: 60 µl & ERA 0319-14-05: 60 µl Pct Recovery = 63% Analysis Date = 07/26/14 SpikeMix = ERA 0319-14-05: 60 µl & ERA 0318-14-02: 60 µl Pct Recovery = 86% Analysis Date = 07/12/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 63% Analysis Date = 06/22/14 SpikeMix = Abs 041814: 60 µl & Abs 041614: 60 µl Pct Recovery = 84% Analysis Date = 05/21/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 69% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-08: 40 µl & Abs 052215: 40 µl Pct Recovery = 83% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 80% Analysis Date = 11/04/15 SpikeMix = ERA 0406-15-07A: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 77% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-08: 40 µl & ERA 0406-15-09: 40 µl Pct Recovery = 71% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 58% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 50% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-07A: 40 µl & Abs 051315: 40 µl Pct Recovery = 61% Analysis Date = 07/31/15 SpikeMix = Abs 051315: 40 µl & Abs 052215: 40 µl Pct Recovery = 63% Analysis Date = 07/30/15 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 82% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 62% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 66% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 59% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 68% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 61% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 66% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 70% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 72% Analysis Date = 04/10/15 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 49% Analysis Date = 11/04/14 SpikeMix = Abs 041714: 8 µl & ERA 0319-14-05: 8 µl Pct Recovery = 78% Analysis Date = 11/04/14 SpikeMix = Abs 041814: 8 µl & ERA 0318-14-02: 8 µl Pct Recovery = 79% Analysis Date = 10/24/14 SpikeMix = ERA 0319-14-05: 8 µl & Abs 041614: 8 µl Pct Recovery = 86% Analysis Date = 10/11/14 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 54% Analysis Date = 10/10/14 SpikeMix = Abs 041714: 30 µl & Abs 041814: 30 µl Pct Recovery = 64% Analysis Date = 10/10/14 SpikeMix = Abs 041814: 30 µl & ERA 0318-14-02: 30 µl Pct Recovery = 62% Analysis Date = 08/30/14 SpikeMix = ERA 0318-14-02: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 83% Analysis Date = 08/16/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 36% Analysis Date = 07/13/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 69% Analysis Date = 07/13/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 65% Analysis Date = 05/30/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 62% Analysis Date = 04/27/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 100% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 71% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-08: 20 µl & ERA 0406-15-09: 20 µl Pct Recovery = 64% Analysis Date = 11/25/15 SpikeMix = Abs 050115: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 84% Analysis Date = 09/15/15 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 75% Analysis Date = 02/23/16 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 65% Analysis Date = 08/11/15 SpikeMix = Abs 050115: 20 µl & Abs 051315: 20 µl Pct Recovery = 52% Analysis Date = 06/26/15 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 79% Analysis Date = 06/09/15 SpikeMix = Abs 051315: 20 µl & Abs 050115: 20 µl Pct Recovery = 60% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 76% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 74% Analysis Date = 11/18/16 SpikeMix = ERA 04281604: 80 µl & ERA 04281603: 80 µl Pct Recovery = 77% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & ERA 04281604: 80 µl Pct Recovery = 71% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 69% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 80% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 102% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 110% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 84% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 83% Analysis Date = 04/09/16 SpikeMix = Abs 051315: 10 µl & ERA 0406-15-09: 10 µl Pct Recovery = 45% Analysis Date = 04/09/16 SpikeMix = Abs 051315: 10 µl & ERA 0406-15-09: 10 µl Pct Recovery = 49% Analysis Date = 01/04/17 Pct Recovery = 82% Analysis Date = 12/31/16 Pct Recovery = 82% Analysis Date = 12/31/16 Pct Recovery = 82% Analysis Date = 12/26/16 Pct Recovery = 82% Analysis Date = 12/26/16 Pct Recovery = 82% Analysis Date = 12/21/16 Pct Recovery = 81% Analysis Date = 12/21/16 Pct Recovery = 81% Analysis Date = 12/16/16 Pct Recovery = 81% Analysis Date = 12/16/16 Pct Recovery = 81% Analysis Date = 12/11/16 Pct Recovery = 81% Analysis Date = 12/11/16 Pct Recovery = 81% Analysis Date = 12/07/16 Pct Recovery = 81% Analysis Date = 12/07/16 Pct Recovery = 81% Analysis Date = 12/02/16 Pct Recovery = 80% Analysis Date = 12/02/16 Pct Recovery = 80% Analysis Date = 11/27/16 Pct Recovery = 80% Analysis Date = 11/27/16 Pct Recovery = 80% Analysis Date = 11/22/16 Pct Recovery = 80% Analysis Date = 11/22/16 Pct Recovery = 80% Analysis Date = 11/17/16 Pct Recovery = 79% Analysis Date = 11/17/16 Pct Recovery = 79% Analysis Date = 11/13/16 Pct Recovery = 79% Analysis Date = 11/13/16 Pct Recovery = 79% Analysis Date = 11/08/16 Pct Recovery = 79% Analysis Date = 11/08/16 Pct Recovery = 79% Analysis Date = 11/03/16 Pct Recovery = 79% Analysis Date = 11/03/16 Pct Recovery = 79% Analysis Date = 10/29/16 Pct Recovery = 78% Analysis Date = 10/29/16 Pct Recovery = 78% Analysis Date = 10/24/16 Pct Recovery = 78% Analysis Date = 10/24/16 Pct Recovery = 78% Analysis Date = 10/20/16 Pct Recovery = 78% Analysis Date = 10/20/16 Pct Recovery = 78% Analysis Date = 10/15/16 Pct Recovery = 78% Analysis Date = 10/15/16 Pct Recovery = 78% Analysis Date = 10/10/16 Pct Recovery = 77% Analysis Date = 10/10/16 Pct Recovery = 77% Analysis Date = 10/05/16 Pct Recovery = 77% Analysis Date = 10/05/16 Pct Recovery = 77% Analysis Date = 09/30/16 Pct Recovery = 77% Analysis Date = 09/30/16 Pct Recovery = 77% Analysis Date = 09/26/16 Pct Recovery = 76% Analysis Date = 09/26/16 Pct Recovery = 76% Analysis Date = 09/21/16 Pct Recovery = 76% Analysis Date = 09/21/16 Pct Recovery = 76% Analysis Date = 09/16/16 Pct Recovery = 76% Analysis Date = 09/16/16 Pct Recovery = 76% Analysis Date = 09/11/16 Pct Recovery = 76% Analysis Date = 09/11/16 Pct Recovery = 76% Analysis Date = 09/06/16 Pct Recovery = 75% Analysis Date = 09/06/16 Pct Recovery = 75% Analysis Date = 09/02/16 Pct Recovery = 75% Analysis Date = 09/02/16 Pct Recovery = 75% Analysis Date = 08/28/16 Pct Recovery = 75% Analysis Date = 08/28/16 Pct Recovery = 75% Analysis Date = 08/23/16 Pct Recovery = 75% Analysis Date = 08/23/16 Pct Recovery = 75% Analysis Date = 08/18/16 Pct Recovery = 74% Analysis Date = 08/18/16 Pct Recovery = 74% Analysis Date = 08/13/16 Pct Recovery = 74% Analysis Date = 08/13/16 Pct Recovery = 74% Analysis Date = 08/09/16 Pct Recovery = 74% Analysis Date = 08/09/16 Pct Recovery = 74% Analysis Date = 08/04/16 Pct Recovery = 74% Analysis Date = 08/04/16 Pct Recovery = 74% Analysis Date = 07/30/16 Pct Recovery = 73% Analysis Date = 07/30/16 Pct Recovery = 73% Analysis Date = 07/25/16 Pct Recovery = 73% Analysis Date = 07/25/16 Pct Recovery = 73% Analysis Date = 07/20/16 Pct Recovery = 73% Analysis Date = 07/20/16 Pct Recovery = 73% Analysis Date = 07/16/16 Pct Recovery = 73% Analysis Date = 07/16/16 Pct Recovery = 73% Analysis Date = 07/11/16 Pct Recovery = 73% Analysis Date = 07/11/16 Pct Recovery = 73% Analysis Date = 07/06/16 Pct Recovery = 73% Analysis Date = 07/06/16 Pct Recovery = 73% Analysis Date = 07/01/16 Pct Recovery = 73% Analysis Date = 07/01/16 Pct Recovery = 73% Analysis Date = 06/26/16 Pct Recovery = 73% Analysis Date = 06/26/16 Pct Recovery = 73% Analysis Date = 06/22/16 Pct Recovery = 73% Analysis Date = 06/22/16 Pct Recovery = 73% Analysis Date = 06/17/16 Pct Recovery = 73% Analysis Date = 06/17/16 Pct Recovery = 73% Analysis Date = 06/12/16 Pct Recovery = 73% Analysis Date = 06/12/16 Pct Recovery = 73% Analysis Date = 06/07/16 Pct Recovery = 73% Analysis Date = 06/07/16 Pct Recovery = 73% Analysis Date = 06/02/16 Pct Recovery = 73% Analysis Date = 06/02/16 Pct Recovery = 73% Analysis Date = 05/29/16 Pct Recovery = 72% Analysis Date = 05/29/16 Pct Recovery = 72% Analysis Date = 05/24/16 Pct Recovery = 72% Analysis Date = 05/24/16 Pct Recovery = 72% Analysis Date = 05/19/16 Pct Recovery = 72% Analysis Date = 05/19/16 Pct Recovery = 72% Analysis Date = 05/14/16 Pct Recovery = 72% Analysis Date = 05/14/16 Pct Recovery = 72% Analysis Date = 05/09/16 Pct Recovery = 72% Analysis Date = 05/09/16 Pct Recovery = 72% Analysis Date = 05/05/16 Pct Recovery = 72% Analysis Date = 05/05/16 Pct Recovery = 72% Analysis Date = 04/30/16 Pct Recovery = 72% Analysis Date = 04/30/16 Pct Recovery = 72% Analysis Date = 04/25/16 Pct Recovery = 72% Analysis Date = 04/25/16 Pct Recovery = 72% Analysis Date = 04/20/16 Pct Recovery = 72% Analysis Date = 04/20/16 Pct Recovery = 72% Analysis Date = 04/15/16 Pct Recovery = 72% Analysis Date = 04/15/16 Pct Recovery = 72% Analysis Date = 04/11/16 Pct Recovery = 72% Analysis Date = 04/11/16 Pct Recovery = 72% Analysis Date = 04/06/16 Pct Recovery = 72% Analysis Date = 04/06/16 Pct Recovery = 72% Analysis Date = 04/01/16 Pct Recovery = 72% Analysis Date = 04/01/16 Pct Recovery = 72% Analysis Date = 03/27/16 Pct Recovery = 72% Analysis Date = 03/27/16 Pct Recovery = 72% Analysis Date = 03/22/16 Pct Recovery = 72% Analysis Date = 03/22/16 Pct Recovery = 72% Analysis Date = 03/18/16 Pct Recovery = 72% Analysis Date = 03/18/16 Pct Recovery = 72% Analysis Date = 03/13/16 Pct Recovery = 72% Analysis Date = 03/13/16 Pct Recovery = 72% Analysis Date = 03/08/16 Pct Recovery = 72% Analysis Date = 03/08/16 Pct Recovery = 72% Analysis Date = 03/03/16 Pct Recovery = 72% Analysis Date = 03/03/16 Pct Recovery = 72% Analysis Date = 02/27/16 Pct Recovery = 72% Analysis Date = 02/27/16 Pct Recovery = 72% Analysis Date = 02/23/16 Pct Recovery = 72% Analysis Date = 02/23/16 Pct Recovery = 72% Analysis Date = 02/18/16 Pct Recovery = 72% Analysis Date = 02/18/16 Pct Recovery = 72% Analysis Date = 02/13/16 Pct Recovery = 72% Analysis Date = 02/13/16 Pct Recovery = 72% Analysis Date = 02/08/16 Pct Recovery = 72% Analysis Date = 02/08/16 Pct Recovery = 72% Analysis Date = 02/03/16 Pct Recovery = 72% Analysis Date = 02/03/16 Pct Recovery = 72% Analysis Date = 01/30/16 Pct Recovery = 72% Analysis Date = 01/30/16 Pct Recovery = 72% Analysis Date = 01/25/16 Pct Recovery = 72% Analysis Date = 01/25/16 Pct Recovery = 72% Analysis Date = 01/20/16 Pct Recovery = 72% Analysis Date = 01/20/16 Pct Recovery = 72% Analysis Date = 01/15/16 Pct Recovery = 72% Analysis Date = 01/15/16 Pct Recovery = 72% Analysis Date = 01/10/16 Pct Recovery = 72% Analysis Date = 01/10/16 Pct Recovery = 72% Analysis Date = 01/06/16 Pct Recovery = 72% Analysis Date = 01/06/16 Pct Recovery = 72% Analysis Date = 01/01/16 Pct Recovery = 72% Analysis Date = 01/01/16 Pct Recovery = 72% Analysis Date = 12/27/15 Pct Recovery = 72% Analysis Date = 12/27/15 Pct Recovery = 72% Analysis Date = 12/22/15 Pct Recovery = 72% Analysis Date = 12/22/15 Pct Recovery = 72% Analysis Date = 12/17/15 Pct Recovery = 72% Analysis Date = 12/17/15 Pct Recovery = 72% Analysis Date = 12/13/15 Pct Recovery = 72% Analysis Date = 12/13/15 Pct Recovery = 72% Analysis Date = 12/08/15 Pct Recovery = 72% Analysis Date = 12/08/15 Pct Recovery = 72% Analysis Date = 12/03/15 Pct Recovery = 72% Analysis Date = 12/03/15 Pct Recovery = 72% Analysis Date = 11/28/15 Pct Recovery = 72% Analysis Date = 11/28/15 Pct Recovery = 72% Analysis Date = 11/23/15 Pct Recovery = 72% Analysis Date = 11/23/15 Pct Recovery = 72% Analysis Date = 11/19/15 Pct Recovery = 72% Analysis Date = 11/19/15 Pct Recovery = 72% Analysis Date = 11/14/15 Pct Recovery = 72% Analysis Date = 11/14/15 Pct Recovery = 72% Analysis Date = 11/09/15 Pct Recovery = 72% Analysis Date = 11/09/15 Pct Recovery = 72% Analysis Date = 11/04/15 Pct Recovery = 72% Analysis Date = 11/04/15 Pct Recovery = 72% Analysis Date = 10/30/15 Pct Recovery = 72% Analysis Date = 10/30/15 Pct Recovery = 72% Analysis Date = 10/26/15 Pct Recovery = 72% Analysis Date = 10/26/15 Pct Recovery = 72% Analysis Date = 10/21/15 Pct Recovery = 72% Analysis Date = 10/21/15 Pct Recovery = 72% Analysis Date = 10/16/15 Pct Recovery = 72% Analysis Date = 10/16/15 Pct Recovery = 72% Analysis Date = 10/11/15 Pct Recovery = 72% Analysis Date = 10/11/15 Pct Recovery = 72% Analysis Date = 10/06/15 Pct Recovery = 72% Analysis Date = 10/06/15 Pct Recovery = 72% Analysis Date = 10/02/15 Pct Recovery = 72% Analysis Date = 10/02/15 Pct Recovery = 72% Analysis Date = 09/27/15 Pct Recovery = 72% Analysis Date = 09/27/15 Pct Recovery = 72% Analysis Date = 09/22/15 Pct Recovery = 72% Analysis Date = 09/22/15 Pct Recovery = 72% Analysis Date = 09/17/15 Pct Recovery = 72% Analysis Date = 09/17/15 Pct Recovery = 72% Analysis Date = 09/12/15 Pct Recovery = 72% Analysis Date = 09/12/15 Pct Recovery = 72% Analysis Date = 09/08/15 Pct Recovery = 72% Analysis Date = 09/08/15 Pct Recovery = 72% Analysis Date = 09/03/15 Pct Recovery = 72% Analysis Date = 09/03/15 Pct Recovery = 72% Analysis Date = 08/29/15 Pct Recovery = 73% Analysis Date = 08/29/15 Pct Recovery = 73% Analysis Date = 08/24/15 Pct Recovery = 73% Analysis Date = 08/24/15 Pct Recovery = 73% Analysis Date = 08/19/15 Pct Recovery = 73% Analysis Date = 08/19/15 Pct Recovery = 73% Analysis Date = 08/15/15 Pct Recovery = 73% Analysis Date = 08/15/15 Pct Recovery = 73% Analysis Date = 08/10/15 Pct Recovery = 73% Analysis Date = 08/10/15 Pct Recovery = 73% Analysis Date = 08/05/15 Pct Recovery = 73% Analysis Date = 08/05/15 Pct Recovery = 73% Analysis Date = 07/31/15 Pct Recovery = 73% Analysis Date = 07/31/15 Pct Recovery = 73% Analysis Date = 07/26/15 Pct Recovery = 73% Analysis Date = 07/26/15 Pct Recovery = 73% Analysis Date = 07/22/15 Pct Recovery = 73% Analysis Date = 07/22/15 Pct Recovery = 73% Analysis Date = 07/17/15 Pct Recovery = 73% Analysis Date = 07/17/15 Pct Recovery = 73% Analysis Date = 07/12/15 Pct Recovery = 73% Analysis Date = 07/12/15 Pct Recovery = 73% Analysis Date = 07/07/15 Pct Recovery = 73% Analysis Date = 07/07/15 Pct Recovery = 73% Analysis Date = 07/02/15 Pct Recovery = 73% Analysis Date = 07/02/15 Pct Recovery = 73% Analysis Date = 06/28/15 Pct Recovery = 73% Analysis Date = 06/28/15 Pct Recovery = 73% Analysis Date = 06/23/15 Pct Recovery = 73% Analysis Date = 06/23/15 Pct Recovery = 73% Analysis Date = 06/18/15 Pct Recovery = 73% Analysis Date = 06/18/15 Pct Recovery = 73% Analysis Date = 06/13/15 Pct Recovery = 73% Analysis Date = 06/13/15 Pct Recovery = 73% Analysis Date = 06/08/15 Pct Recovery = 73% Analysis Date = 06/08/15 Pct Recovery = 73% Analysis Date = 06/04/15 Pct Recovery = 73% Analysis Date = 06/04/15 Pct Recovery = 73% Analysis Date = 05/30/15 Pct Recovery = 73% Analysis Date = 05/30/15 Pct Recovery = 73% Analysis Date = 05/25/15 Pct Recovery = 73% Analysis Date = 05/25/15 Pct Recovery = 73% Analysis Date = 05/20/15 Pct Recovery = 73% Analysis Date = 05/20/15 Pct Recovery = 73% Analysis Date = 05/15/15 Pct Recovery = 73% Analysis Date = 05/15/15 Pct Recovery = 73% Analysis Date = 05/11/15 Pct Recovery = 73% Analysis Date = 05/11/15 Pct Recovery = 73% Analysis Date = 05/06/15 Pct Recovery = 73% Analysis Date = 05/06/15 Pct Recovery = 73% Analysis Date = 05/01/15 Pct Recovery = 73% Analysis Date = 05/01/15 Pct Recovery = 73% Analysis Date = 04/26/15 Pct Recovery = 73% Analysis Date = 04/26/15 Pct Recovery = 73% Analysis Date = 04/21/15 Pct Recovery = 73% Analysis Date = 04/21/15 Pct Recovery = 73% Analysis Date = 04/17/15 Pct Recovery = 73% Analysis Date = 04/17/15 Pct Recovery = 73% Analysis Date = 04/12/15 Pct Recovery = 73% Analysis Date = 04/12/15 Pct Recovery = 73% Analysis Date = 04/07/15 Pct Recovery = 73% Analysis Date = 04/07/15 Pct Recovery = 73% Analysis Date = 04/02/15 Pct Recovery = 73% Analysis Date = 04/02/15 Pct Recovery = 73% Analysis Date = 03/28/15 Pct Recovery = 73% Analysis Date = 03/28/15 Pct Recovery = 73% Analysis Date = 03/24/15 Pct Recovery = 72% Analysis Date = 03/24/15 Pct Recovery = 72% Analysis Date = 03/19/15 Pct Recovery = 72% Analysis Date = 03/19/15 Pct Recovery = 72% Analysis Date = 03/14/15 Pct Recovery = 72% Analysis Date = 03/14/15 Pct Recovery = 72% Analysis Date = 03/09/15 Pct Recovery = 72% Analysis Date = 03/09/15 Pct Recovery = 72% Analysis Date = 03/04/15 Pct Recovery = 72% Analysis Date = 03/04/15 Pct Recovery = 72% Analysis Date = 02/28/15 Pct Recovery = 72% Analysis Date = 02/28/15 Pct Recovery = 72% Analysis Date = 02/23/15 Pct Recovery = 72% Analysis Date = 02/23/15 Pct Recovery = 72% Analysis Date = 02/18/15 Pct Recovery = 72% Analysis Date = 02/18/15 Pct Recovery = 72% Analysis Date = 02/13/15 Pct Recovery = 72% Analysis Date = 02/13/15 Pct Recovery = 72% Analysis Date = 02/08/15 Pct Recovery = 72% Analysis Date = 02/08/15 Pct Recovery = 72% Analysis Date = 02/04/15 Pct Recovery = 72% Analysis Date = 02/04/15 Pct Recovery = 72% Analysis Date = 01/30/15 Pct Recovery = 72% Analysis Date = 01/30/15 Pct Recovery = 72% Analysis Date = 01/25/15 Pct Recovery = 72% Analysis Date = 01/25/15 Pct Recovery = 72% Analysis Date = 01/20/15 Pct Recovery = 72% Analysis Date = 01/20/15 Pct Recovery = 72% Analysis Date = 01/15/15 Pct Recovery = 72% Analysis Date = 01/15/15 Pct Recovery = 72% Analysis Date = 01/11/15 Pct Recovery = 71% Analysis Date = 01/11/15 Pct Recovery = 71% Analysis Date = 01/06/15 Pct Recovery = 71% Analysis Date = 01/06/15 Pct Recovery = 71% Analysis Date = 01/01/15 Pct Recovery = 71% Analysis Date = 01/01/15 Pct Recovery = 71% Analysis Date = 12/27/14 Pct Recovery = 71% Analysis Date = 12/27/14 Pct Recovery = 71% Analysis Date = 12/22/14 Pct Recovery = 71% Analysis Date = 12/22/14 Pct Recovery = 71% Analysis Date = 12/18/14 Pct Recovery = 71% Analysis Date = 12/18/14 Pct Recovery = 71% Analysis Date = 12/13/14 Pct Recovery = 71% Analysis Date = 12/13/14 Pct Recovery = 71% Analysis Date = 12/08/14 Pct Recovery = 71% Analysis Date = 12/08/14 Pct Recovery = 71% Analysis Date = 12/03/14 Pct Recovery = 71% Analysis Date = 12/03/14 Pct Recovery = 71% Analysis Date = 11/28/14 Pct Recovery = 71% Analysis Date = 11/28/14 Pct Recovery = 71% Analysis Date = 11/24/14 Pct Recovery = 71% Analysis Date = 11/24/14 Pct Recovery = 71% Analysis Date = 11/19/14 Pct Recovery = 71% Analysis Date = 11/19/14 Pct Recovery = 71% Analysis Date = 11/14/14 Pct Recovery = 71% Analysis Date = 11/14/14 Pct Recovery = 71% Analysis Date = 11/09/14 Pct Recovery = 71% Analysis Date = 11/09/14 Pct Recovery = 71% Analysis Date = 11/04/14 Pct Recovery = 71% Analysis Date = 11/04/14 Pct Recovery = 71% Analysis Date = 10/31/14 Pct Recovery = 71% Analysis Date = 10/31/14 Pct Recovery = 71% Analysis Date = 10/26/14 Pct Recovery = 71% Analysis Date = 10/26/14 Pct Recovery = 71% Analysis Date = 10/21/14 Pct Recovery = 71% Analysis Date = 10/21/14 Pct Recovery = 71% Analysis Date = 10/16/14 Pct Recovery = 71% Analysis Date = 10/16/14 Pct Recovery = 71% Analysis Date = 10/11/14 Pct Recovery = 71% Analysis Date = 10/11/14 Pct Recovery = 71% Analysis Date = 10/07/14 Pct Recovery = 71% Analysis Date = 10/07/14 Pct Recovery = 71% Analysis Date = 10/02/14 Pct Recovery = 71% Analysis Date = 10/02/14 Pct Recovery = 71% Analysis Date = 09/27/14 Pct Recovery = 70% Analysis Date = 09/27/14 Pct Recovery = 70% Analysis Date = 09/22/14 Pct Recovery = 70% Analysis Date = 09/22/14 Pct Recovery = 70% Analysis Date = 09/17/14 Pct Recovery = 70% Analysis Date = 09/17/14 Pct Recovery = 70% Analysis Date = 09/13/14 Pct Recovery = 70% Analysis Date = 09/13/14 Pct Recovery = 70% Analysis Date = 09/08/14 Pct Recovery = 70% Analysis Date = 09/08/14 Pct Recovery = 70% Analysis Date = 09/03/14 Pct Recovery = 70% Analysis Date = 09/03/14 Pct Recovery = 70% Analysis Date = 08/29/14 Pct Recovery = 70% Analysis Date = 08/29/14 Pct Recovery = 70% Analysis Date = 08/24/14 Pct Recovery = 70% Analysis Date = 08/24/14 Pct Recovery = 70% Analysis Date = 08/20/14 Pct Recovery = 70% Analysis Date = 08/20/14 Pct Recovery = 70% Analysis Date = 08/15/14 Pct Recovery = 70% Analysis Date = 08/15/14 Pct Recovery = 70% Analysis Date = 08/10/14 Pct Recovery = 70% Analysis Date = 08/10/14 Pct Recovery = 70% Analysis Date = 08/05/14 Pct Recovery = 70% Analysis Date = 08/05/14 Pct Recovery = 70% Analysis Date = 07/31/14 Pct Recovery = 70% Analysis Date = 07/31/14 Pct Recovery = 70% Analysis Date = 07/27/14 Pct Recovery = 70% Analysis Date = 07/27/14 Pct Recovery = 70% Analysis Date = 07/22/14 Pct Recovery = 70% Analysis Date = 07/22/14 Pct Recovery = 70% Analysis Date = 07/17/14 Pct Recovery = 70% Analysis Date = 07/17/14 Pct Recovery = 70% Analysis Date = 07/12/14 Pct Recovery = 70% Analysis Date = 07/12/14 Pct Recovery = 70% Analysis Date = 07/07/14 Pct Recovery = 70% Analysis Date = 07/07/14 Pct Recovery = 70% Analysis Date = 07/03/14 Pct Recovery = 70% Analysis Date = 07/03/14 Pct Recovery = 70% Analysis Date = 06/28/14 Pct Recovery = 69% Analysis Date = 06/28/14 Pct Recovery = 69% Analysis Date = 06/23/14 Pct Recovery = 69% Analysis Date = 06/23/14 Pct Recovery = 69% Analysis Date = 06/18/14 Pct Recovery = 69% Analysis Date = 06/18/14 Pct Recovery = 69% Analysis Date = 06/13/14 Pct Recovery = 69% Analysis Date = 06/13/14 Pct Recovery = 69% Analysis Date = 06/09/14 Pct Recovery = 69% Analysis Date = 06/09/14 Pct Recovery = 69% Analysis Date = 06/04/14 Pct Recovery = 69% Analysis Date = 06/04/14 Pct Recovery = 69% Analysis Date = 05/30/14 Pct Recovery = 69% Analysis Date = 05/30/14 Pct Recovery = 69% Analysis Date = 05/25/14 Pct Recovery = 69% Analysis Date = 05/25/14 Pct Recovery = 69% Analysis Date = 05/21/14 Pct Recovery = 69% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
DESVENLAFAXINE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 12 77% 18% 77% 10%
>= Reporting Level 61 72% 13% 71% 14%
Total 73 73% 14% 72% 14%

Sample Statistics
DESVENLAFAXINE

Characteristic N % % Basis
Plotted 73 97% Spiked
Estimated Values 11 15% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 1 1% Spiked
Spiked 75 .  
False Negatives 1 1% 1 out of 75
Not Spiked 40 .  
False Positives 0 0% 0 out of 40

BQS OBSP Determination:
DEXTROMETHORPHAN
METHOD: 2440 , TESTIDCODE: 67468LCM56
Open Data Set

Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 66% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 59% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 80 µl & ERA 0406-15-08: 80 µl Pct Recovery = 62% Analysis Date = 11/24/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 79% Analysis Date = 11/05/15 SpikeMix = ERA 0406-15-08: 80 µl & Abs 052215: 80 µl Pct Recovery = 65% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 80 µl & Abs 051315: 80 µl Pct Recovery = 78% Analysis Date = 10/01/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 82% Analysis Date = 11/18/16 SpikeMix = ERA 04281604: 80 µl & ERA 04281603: 80 µl Pct Recovery = 56% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & ERA 04281604: 80 µl Pct Recovery = 52% Analysis Date = 09/24/16 SpikeMix = Crescent EN160610015: 80 µl & Abs 061416: 80 µl Pct Recovery = 64% Analysis Date = 09/24/16 SpikeMix = Abs 061416: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 65% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 81% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 84% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 78% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 79% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-04: 15 µl & Abs 041814: 15 µl Pct Recovery = 61% Analysis Date = 02/06/15 SpikeMix = Abs 041814: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 66% Analysis Date = 07/12/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 65% Analysis Date = 06/22/14 SpikeMix = Abs 041814: 60 µl & Abs 041614: 60 µl Pct Recovery = 77% Analysis Date = 05/21/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 65% Analysis Date = 05/07/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 74% Analysis Date = 04/29/15 SpikeMix = ERA 0319-14-05: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 84% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 71% Analysis Date = 01/16/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 86% Analysis Date = 12/07/14 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 72% Analysis Date = 12/06/14 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 67% Analysis Date = 08/28/14 SpikeMix = ERA 0319-14-04: 60 µl & ERA 0319-14-05: 60 µl Pct Recovery = 56% Analysis Date = 07/26/14 SpikeMix = ERA 0319-14-05: 60 µl & ERA 0318-14-02: 60 µl Pct Recovery = 81% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 63% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 58% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-08: 40 µl & Abs 052215: 40 µl Pct Recovery = 68% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 55% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-07A: 40 µl & Abs 051315: 40 µl Pct Recovery = 57% Analysis Date = 11/04/15 SpikeMix = ERA 0406-15-07A: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 58% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-08: 40 µl & ERA 0406-15-09: 40 µl Pct Recovery = 66% Analysis Date = 07/31/15 SpikeMix = Abs 051315: 40 µl & Abs 052215: 40 µl Pct Recovery = 55% Analysis Date = 07/30/15 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 72% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 74% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 97% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 71% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 71% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 58% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 57% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 53% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 61% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 55% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 59% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 41% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 51% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 44% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 55% Analysis Date = 04/10/15 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 51% Analysis Date = 11/04/14 SpikeMix = Abs 041814: 8 µl & ERA 0318-14-02: 8 µl Pct Recovery = 47% Analysis Date = 10/11/14 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 54% Analysis Date = 11/04/14 SpikeMix = Abs 041714: 8 µl & ERA 0319-14-05: 8 µl Pct Recovery = 50% Analysis Date = 10/24/14 SpikeMix = ERA 0319-14-05: 8 µl & Abs 041614: 8 µl Pct Recovery = 72% Analysis Date = 10/10/14 SpikeMix = Abs 041714: 30 µl & Abs 041814: 30 µl Pct Recovery = 54% Analysis Date = 10/10/14 SpikeMix = Abs 041814: 30 µl & ERA 0318-14-02: 30 µl Pct Recovery = 59% Analysis Date = 07/13/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 62% Analysis Date = 05/30/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 69% Analysis Date = 08/30/14 SpikeMix = ERA 0318-14-02: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 69% Analysis Date = 08/16/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 30% Analysis Date = 07/13/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 41% Analysis Date = 04/27/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 77% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 54% Analysis Date = 02/23/16 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 62% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-08: 20 µl & ERA 0406-15-09: 20 µl Pct Recovery = 51% Analysis Date = 11/25/15 SpikeMix = Abs 050115: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 71% Analysis Date = 09/15/15 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 65% Analysis Date = 09/09/15 SpikeMix = ERA 0406-15-08: 20 µl & Abs 052215: 20 µl Pct Recovery = 78% Analysis Date = 08/11/15 SpikeMix = Abs 050115: 20 µl & Abs 051315: 20 µl Pct Recovery = 44% Analysis Date = 06/26/15 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 60% Analysis Date = 06/09/15 SpikeMix = Abs 051315: 20 µl & Abs 050115: 20 µl Pct Recovery = 60% Analysis Date = 04/09/16 SpikeMix = Abs 051315: 10 µl & ERA 0406-15-09: 10 µl Pct Recovery = 40% Analysis Date = 04/09/16 SpikeMix = Abs 051315: 10 µl & ERA 0406-15-09: 10 µl Pct Recovery = 59% Analysis Date = 01/04/17 Pct Recovery = 65% Analysis Date = 12/31/16 Pct Recovery = 65% Analysis Date = 12/31/16 Pct Recovery = 65% Analysis Date = 12/26/16 Pct Recovery = 65% Analysis Date = 12/26/16 Pct Recovery = 65% Analysis Date = 12/21/16 Pct Recovery = 65% Analysis Date = 12/21/16 Pct Recovery = 65% Analysis Date = 12/16/16 Pct Recovery = 65% Analysis Date = 12/16/16 Pct Recovery = 65% Analysis Date = 12/11/16 Pct Recovery = 65% Analysis Date = 12/11/16 Pct Recovery = 65% Analysis Date = 12/07/16 Pct Recovery = 65% Analysis Date = 12/07/16 Pct Recovery = 65% Analysis Date = 12/02/16 Pct Recovery = 65% Analysis Date = 12/02/16 Pct Recovery = 65% Analysis Date = 11/27/16 Pct Recovery = 65% Analysis Date = 11/27/16 Pct Recovery = 65% Analysis Date = 11/22/16 Pct Recovery = 65% Analysis Date = 11/22/16 Pct Recovery = 65% Analysis Date = 11/17/16 Pct Recovery = 64% Analysis Date = 11/17/16 Pct Recovery = 64% Analysis Date = 11/13/16 Pct Recovery = 64% Analysis Date = 11/13/16 Pct Recovery = 64% Analysis Date = 11/08/16 Pct Recovery = 64% Analysis Date = 11/08/16 Pct Recovery = 64% Analysis Date = 11/03/16 Pct Recovery = 64% Analysis Date = 11/03/16 Pct Recovery = 64% Analysis Date = 10/29/16 Pct Recovery = 64% Analysis Date = 10/29/16 Pct Recovery = 64% Analysis Date = 10/24/16 Pct Recovery = 64% Analysis Date = 10/24/16 Pct Recovery = 64% Analysis Date = 10/20/16 Pct Recovery = 64% Analysis Date = 10/20/16 Pct Recovery = 64% Analysis Date = 10/15/16 Pct Recovery = 64% Analysis Date = 10/15/16 Pct Recovery = 64% Analysis Date = 10/10/16 Pct Recovery = 64% Analysis Date = 10/10/16 Pct Recovery = 64% Analysis Date = 10/05/16 Pct Recovery = 64% Analysis Date = 10/05/16 Pct Recovery = 64% Analysis Date = 09/30/16 Pct Recovery = 64% Analysis Date = 09/30/16 Pct Recovery = 64% Analysis Date = 09/26/16 Pct Recovery = 63% Analysis Date = 09/26/16 Pct Recovery = 63% Analysis Date = 09/21/16 Pct Recovery = 63% Analysis Date = 09/21/16 Pct Recovery = 63% Analysis Date = 09/16/16 Pct Recovery = 63% Analysis Date = 09/16/16 Pct Recovery = 63% Analysis Date = 09/11/16 Pct Recovery = 63% Analysis Date = 09/11/16 Pct Recovery = 63% Analysis Date = 09/06/16 Pct Recovery = 63% Analysis Date = 09/06/16 Pct Recovery = 63% Analysis Date = 09/02/16 Pct Recovery = 63% Analysis Date = 09/02/16 Pct Recovery = 63% Analysis Date = 08/28/16 Pct Recovery = 63% Analysis Date = 08/28/16 Pct Recovery = 63% Analysis Date = 08/23/16 Pct Recovery = 63% Analysis Date = 08/23/16 Pct Recovery = 63% Analysis Date = 08/18/16 Pct Recovery = 63% Analysis Date = 08/18/16 Pct Recovery = 63% Analysis Date = 08/13/16 Pct Recovery = 63% Analysis Date = 08/13/16 Pct Recovery = 63% Analysis Date = 08/09/16 Pct Recovery = 63% Analysis Date = 08/09/16 Pct Recovery = 63% Analysis Date = 08/04/16 Pct Recovery = 63% Analysis Date = 08/04/16 Pct Recovery = 63% Analysis Date = 07/30/16 Pct Recovery = 63% Analysis Date = 07/30/16 Pct Recovery = 63% Analysis Date = 07/25/16 Pct Recovery = 63% Analysis Date = 07/25/16 Pct Recovery = 63% Analysis Date = 07/20/16 Pct Recovery = 63% Analysis Date = 07/20/16 Pct Recovery = 63% Analysis Date = 07/16/16 Pct Recovery = 63% Analysis Date = 07/16/16 Pct Recovery = 63% Analysis Date = 07/11/16 Pct Recovery = 63% Analysis Date = 07/11/16 Pct Recovery = 63% Analysis Date = 07/06/16 Pct Recovery = 63% Analysis Date = 07/06/16 Pct Recovery = 63% Analysis Date = 07/01/16 Pct Recovery = 63% Analysis Date = 07/01/16 Pct Recovery = 63% Analysis Date = 06/26/16 Pct Recovery = 63% Analysis Date = 06/26/16 Pct Recovery = 63% Analysis Date = 06/22/16 Pct Recovery = 63% Analysis Date = 06/22/16 Pct Recovery = 63% Analysis Date = 06/17/16 Pct Recovery = 63% Analysis Date = 06/17/16 Pct Recovery = 63% Analysis Date = 06/12/16 Pct Recovery = 63% Analysis Date = 06/12/16 Pct Recovery = 63% Analysis Date = 06/07/16 Pct Recovery = 63% Analysis Date = 06/07/16 Pct Recovery = 63% Analysis Date = 06/02/16 Pct Recovery = 63% Analysis Date = 06/02/16 Pct Recovery = 63% Analysis Date = 05/29/16 Pct Recovery = 62% Analysis Date = 05/29/16 Pct Recovery = 62% Analysis Date = 05/24/16 Pct Recovery = 62% Analysis Date = 05/24/16 Pct Recovery = 62% Analysis Date = 05/19/16 Pct Recovery = 62% Analysis Date = 05/19/16 Pct Recovery = 62% Analysis Date = 05/14/16 Pct Recovery = 62% Analysis Date = 05/14/16 Pct Recovery = 62% Analysis Date = 05/09/16 Pct Recovery = 62% Analysis Date = 05/09/16 Pct Recovery = 62% Analysis Date = 05/05/16 Pct Recovery = 62% Analysis Date = 05/05/16 Pct Recovery = 62% Analysis Date = 04/30/16 Pct Recovery = 62% Analysis Date = 04/30/16 Pct Recovery = 62% Analysis Date = 04/25/16 Pct Recovery = 62% Analysis Date = 04/25/16 Pct Recovery = 62% Analysis Date = 04/20/16 Pct Recovery = 62% Analysis Date = 04/20/16 Pct Recovery = 62% Analysis Date = 04/15/16 Pct Recovery = 62% Analysis Date = 04/15/16 Pct Recovery = 62% Analysis Date = 04/11/16 Pct Recovery = 62% Analysis Date = 04/11/16 Pct Recovery = 62% Analysis Date = 04/06/16 Pct Recovery = 62% Analysis Date = 04/06/16 Pct Recovery = 62% Analysis Date = 04/01/16 Pct Recovery = 63% Analysis Date = 04/01/16 Pct Recovery = 63% Analysis Date = 03/27/16 Pct Recovery = 63% Analysis Date = 03/27/16 Pct Recovery = 63% Analysis Date = 03/22/16 Pct Recovery = 63% Analysis Date = 03/22/16 Pct Recovery = 63% Analysis Date = 03/18/16 Pct Recovery = 63% Analysis Date = 03/18/16 Pct Recovery = 63% Analysis Date = 03/13/16 Pct Recovery = 63% Analysis Date = 03/13/16 Pct Recovery = 63% Analysis Date = 03/08/16 Pct Recovery = 63% Analysis Date = 03/08/16 Pct Recovery = 63% Analysis Date = 03/03/16 Pct Recovery = 63% Analysis Date = 03/03/16 Pct Recovery = 63% Analysis Date = 02/27/16 Pct Recovery = 63% Analysis Date = 02/27/16 Pct Recovery = 63% Analysis Date = 02/23/16 Pct Recovery = 63% Analysis Date = 02/23/16 Pct Recovery = 63% Analysis Date = 02/18/16 Pct Recovery = 63% Analysis Date = 02/18/16 Pct Recovery = 63% Analysis Date = 02/13/16 Pct Recovery = 63% Analysis Date = 02/13/16 Pct Recovery = 63% Analysis Date = 02/08/16 Pct Recovery = 63% Analysis Date = 02/08/16 Pct Recovery = 63% Analysis Date = 02/03/16 Pct Recovery = 64% Analysis Date = 02/03/16 Pct Recovery = 64% Analysis Date = 01/30/16 Pct Recovery = 64% Analysis Date = 01/30/16 Pct Recovery = 64% Analysis Date = 01/25/16 Pct Recovery = 64% Analysis Date = 01/25/16 Pct Recovery = 64% Analysis Date = 01/20/16 Pct Recovery = 64% Analysis Date = 01/20/16 Pct Recovery = 64% Analysis Date = 01/15/16 Pct Recovery = 64% Analysis Date = 01/15/16 Pct Recovery = 64% Analysis Date = 01/10/16 Pct Recovery = 64% Analysis Date = 01/10/16 Pct Recovery = 64% Analysis Date = 01/06/16 Pct Recovery = 64% Analysis Date = 01/06/16 Pct Recovery = 64% Analysis Date = 01/01/16 Pct Recovery = 64% Analysis Date = 01/01/16 Pct Recovery = 64% Analysis Date = 12/27/15 Pct Recovery = 64% Analysis Date = 12/27/15 Pct Recovery = 64% Analysis Date = 12/22/15 Pct Recovery = 64% Analysis Date = 12/22/15 Pct Recovery = 64% Analysis Date = 12/17/15 Pct Recovery = 64% Analysis Date = 12/17/15 Pct Recovery = 64% Analysis Date = 12/13/15 Pct Recovery = 64% Analysis Date = 12/13/15 Pct Recovery = 64% Analysis Date = 12/08/15 Pct Recovery = 64% Analysis Date = 12/08/15 Pct Recovery = 64% Analysis Date = 12/03/15 Pct Recovery = 64% Analysis Date = 12/03/15 Pct Recovery = 64% Analysis Date = 11/28/15 Pct Recovery = 64% Analysis Date = 11/28/15 Pct Recovery = 64% Analysis Date = 11/23/15 Pct Recovery = 64% Analysis Date = 11/23/15 Pct Recovery = 64% Analysis Date = 11/19/15 Pct Recovery = 64% Analysis Date = 11/19/15 Pct Recovery = 64% Analysis Date = 11/14/15 Pct Recovery = 64% Analysis Date = 11/14/15 Pct Recovery = 64% Analysis Date = 11/09/15 Pct Recovery = 64% Analysis Date = 11/09/15 Pct Recovery = 64% Analysis Date = 11/04/15 Pct Recovery = 64% Analysis Date = 11/04/15 Pct Recovery = 64% Analysis Date = 10/30/15 Pct Recovery = 64% Analysis Date = 10/30/15 Pct Recovery = 64% Analysis Date = 10/26/15 Pct Recovery = 64% Analysis Date = 10/26/15 Pct Recovery = 64% Analysis Date = 10/21/15 Pct Recovery = 64% Analysis Date = 10/21/15 Pct Recovery = 64% Analysis Date = 10/16/15 Pct Recovery = 65% Analysis Date = 10/16/15 Pct Recovery = 65% Analysis Date = 10/11/15 Pct Recovery = 65% Analysis Date = 10/11/15 Pct Recovery = 65% Analysis Date = 10/06/15 Pct Recovery = 65% Analysis Date = 10/06/15 Pct Recovery = 65% Analysis Date = 10/02/15 Pct Recovery = 65% Analysis Date = 10/02/15 Pct Recovery = 65% Analysis Date = 09/27/15 Pct Recovery = 65% Analysis Date = 09/27/15 Pct Recovery = 65% Analysis Date = 09/22/15 Pct Recovery = 65% Analysis Date = 09/22/15 Pct Recovery = 65% Analysis Date = 09/17/15 Pct Recovery = 65% Analysis Date = 09/17/15 Pct Recovery = 65% Analysis Date = 09/12/15 Pct Recovery = 65% Analysis Date = 09/12/15 Pct Recovery = 65% Analysis Date = 09/08/15 Pct Recovery = 65% Analysis Date = 09/08/15 Pct Recovery = 65% Analysis Date = 09/03/15 Pct Recovery = 65% Analysis Date = 09/03/15 Pct Recovery = 65% Analysis Date = 08/29/15 Pct Recovery = 65% Analysis Date = 08/29/15 Pct Recovery = 65% Analysis Date = 08/24/15 Pct Recovery = 65% Analysis Date = 08/24/15 Pct Recovery = 65% Analysis Date = 08/19/15 Pct Recovery = 65% Analysis Date = 08/19/15 Pct Recovery = 65% Analysis Date = 08/15/15 Pct Recovery = 65% Analysis Date = 08/15/15 Pct Recovery = 65% Analysis Date = 08/10/15 Pct Recovery = 65% Analysis Date = 08/10/15 Pct Recovery = 65% Analysis Date = 08/05/15 Pct Recovery = 65% Analysis Date = 08/05/15 Pct Recovery = 65% Analysis Date = 07/31/15 Pct Recovery = 65% Analysis Date = 07/31/15 Pct Recovery = 65% Analysis Date = 07/26/15 Pct Recovery = 65% Analysis Date = 07/26/15 Pct Recovery = 65% Analysis Date = 07/22/15 Pct Recovery = 65% Analysis Date = 07/22/15 Pct Recovery = 65% Analysis Date = 07/17/15 Pct Recovery = 65% Analysis Date = 07/17/15 Pct Recovery = 65% Analysis Date = 07/12/15 Pct Recovery = 65% Analysis Date = 07/12/15 Pct Recovery = 65% Analysis Date = 07/07/15 Pct Recovery = 65% Analysis Date = 07/07/15 Pct Recovery = 65% Analysis Date = 07/02/15 Pct Recovery = 65% Analysis Date = 07/02/15 Pct Recovery = 65% Analysis Date = 06/28/15 Pct Recovery = 65% Analysis Date = 06/28/15 Pct Recovery = 65% Analysis Date = 06/23/15 Pct Recovery = 65% Analysis Date = 06/23/15 Pct Recovery = 65% Analysis Date = 06/18/15 Pct Recovery = 65% Analysis Date = 06/18/15 Pct Recovery = 65% Analysis Date = 06/13/15 Pct Recovery = 65% Analysis Date = 06/13/15 Pct Recovery = 65% Analysis Date = 06/08/15 Pct Recovery = 65% Analysis Date = 06/08/15 Pct Recovery = 65% Analysis Date = 06/04/15 Pct Recovery = 65% Analysis Date = 06/04/15 Pct Recovery = 65% Analysis Date = 05/30/15 Pct Recovery = 65% Analysis Date = 05/30/15 Pct Recovery = 65% Analysis Date = 05/25/15 Pct Recovery = 65% Analysis Date = 05/25/15 Pct Recovery = 65% Analysis Date = 05/20/15 Pct Recovery = 65% Analysis Date = 05/20/15 Pct Recovery = 65% Analysis Date = 05/15/15 Pct Recovery = 65% Analysis Date = 05/15/15 Pct Recovery = 65% Analysis Date = 05/11/15 Pct Recovery = 65% Analysis Date = 05/11/15 Pct Recovery = 65% Analysis Date = 05/06/15 Pct Recovery = 65% Analysis Date = 05/06/15 Pct Recovery = 65% Analysis Date = 05/01/15 Pct Recovery = 65% Analysis Date = 05/01/15 Pct Recovery = 65% Analysis Date = 04/26/15 Pct Recovery = 65% Analysis Date = 04/26/15 Pct Recovery = 65% Analysis Date = 04/21/15 Pct Recovery = 65% Analysis Date = 04/21/15 Pct Recovery = 65% Analysis Date = 04/17/15 Pct Recovery = 65% Analysis Date = 04/17/15 Pct Recovery = 65% Analysis Date = 04/12/15 Pct Recovery = 65% Analysis Date = 04/12/15 Pct Recovery = 65% Analysis Date = 04/07/15 Pct Recovery = 65% Analysis Date = 04/07/15 Pct Recovery = 65% Analysis Date = 04/02/15 Pct Recovery = 65% Analysis Date = 04/02/15 Pct Recovery = 65% Analysis Date = 03/28/15 Pct Recovery = 64% Analysis Date = 03/28/15 Pct Recovery = 64% Analysis Date = 03/24/15 Pct Recovery = 64% Analysis Date = 03/24/15 Pct Recovery = 64% Analysis Date = 03/19/15 Pct Recovery = 64% Analysis Date = 03/19/15 Pct Recovery = 64% Analysis Date = 03/14/15 Pct Recovery = 64% Analysis Date = 03/14/15 Pct Recovery = 64% Analysis Date = 03/09/15 Pct Recovery = 64% Analysis Date = 03/09/15 Pct Recovery = 64% Analysis Date = 03/04/15 Pct Recovery = 64% Analysis Date = 03/04/15 Pct Recovery = 64% Analysis Date = 02/28/15 Pct Recovery = 64% Analysis Date = 02/28/15 Pct Recovery = 64% Analysis Date = 02/23/15 Pct Recovery = 64% Analysis Date = 02/23/15 Pct Recovery = 64% Analysis Date = 02/18/15 Pct Recovery = 64% Analysis Date = 02/18/15 Pct Recovery = 64% Analysis Date = 02/13/15 Pct Recovery = 64% Analysis Date = 02/13/15 Pct Recovery = 64% Analysis Date = 02/08/15 Pct Recovery = 64% Analysis Date = 02/08/15 Pct Recovery = 64% Analysis Date = 02/04/15 Pct Recovery = 64% Analysis Date = 02/04/15 Pct Recovery = 64% Analysis Date = 01/30/15 Pct Recovery = 64% Analysis Date = 01/30/15 Pct Recovery = 64% Analysis Date = 01/25/15 Pct Recovery = 64% Analysis Date = 01/25/15 Pct Recovery = 64% Analysis Date = 01/20/15 Pct Recovery = 63% Analysis Date = 01/20/15 Pct Recovery = 63% Analysis Date = 01/15/15 Pct Recovery = 63% Analysis Date = 01/15/15 Pct Recovery = 63% Analysis Date = 01/11/15 Pct Recovery = 63% Analysis Date = 01/11/15 Pct Recovery = 63% Analysis Date = 01/06/15 Pct Recovery = 63% Analysis Date = 01/06/15 Pct Recovery = 63% Analysis Date = 01/01/15 Pct Recovery = 63% Analysis Date = 01/01/15 Pct Recovery = 63% Analysis Date = 12/27/14 Pct Recovery = 63% Analysis Date = 12/27/14 Pct Recovery = 63% Analysis Date = 12/22/14 Pct Recovery = 63% Analysis Date = 12/22/14 Pct Recovery = 63% Analysis Date = 12/18/14 Pct Recovery = 63% Analysis Date = 12/18/14 Pct Recovery = 63% Analysis Date = 12/13/14 Pct Recovery = 63% Analysis Date = 12/13/14 Pct Recovery = 63% Analysis Date = 12/08/14 Pct Recovery = 63% Analysis Date = 12/08/14 Pct Recovery = 63% Analysis Date = 12/03/14 Pct Recovery = 63% Analysis Date = 12/03/14 Pct Recovery = 63% Analysis Date = 11/28/14 Pct Recovery = 63% Analysis Date = 11/28/14 Pct Recovery = 63% Analysis Date = 11/24/14 Pct Recovery = 63% Analysis Date = 11/24/14 Pct Recovery = 63% Analysis Date = 11/19/14 Pct Recovery = 63% Analysis Date = 11/19/14 Pct Recovery = 63% Analysis Date = 11/14/14 Pct Recovery = 63% Analysis Date = 11/14/14 Pct Recovery = 63% Analysis Date = 11/09/14 Pct Recovery = 63% Analysis Date = 11/09/14 Pct Recovery = 63% Analysis Date = 11/04/14 Pct Recovery = 62% Analysis Date = 11/04/14 Pct Recovery = 62% Analysis Date = 10/31/14 Pct Recovery = 62% Analysis Date = 10/31/14 Pct Recovery = 62% Analysis Date = 10/26/14 Pct Recovery = 62% Analysis Date = 10/26/14 Pct Recovery = 62% Analysis Date = 10/21/14 Pct Recovery = 62% Analysis Date = 10/21/14 Pct Recovery = 62% Analysis Date = 10/16/14 Pct Recovery = 62% Analysis Date = 10/16/14 Pct Recovery = 62% Analysis Date = 10/11/14 Pct Recovery = 62% Analysis Date = 10/11/14 Pct Recovery = 62% Analysis Date = 10/07/14 Pct Recovery = 62% Analysis Date = 10/07/14 Pct Recovery = 62% Analysis Date = 10/02/14 Pct Recovery = 62% Analysis Date = 10/02/14 Pct Recovery = 62% Analysis Date = 09/27/14 Pct Recovery = 62% Analysis Date = 09/27/14 Pct Recovery = 62% Analysis Date = 09/22/14 Pct Recovery = 62% Analysis Date = 09/22/14 Pct Recovery = 62% Analysis Date = 09/17/14 Pct Recovery = 62% Analysis Date = 09/17/14 Pct Recovery = 62% Analysis Date = 09/13/14 Pct Recovery = 62% Analysis Date = 09/13/14 Pct Recovery = 62% Analysis Date = 09/08/14 Pct Recovery = 62% Analysis Date = 09/08/14 Pct Recovery = 62% Analysis Date = 09/03/14 Pct Recovery = 62% Analysis Date = 09/03/14 Pct Recovery = 62% Analysis Date = 08/29/14 Pct Recovery = 62% Analysis Date = 08/29/14 Pct Recovery = 62% Analysis Date = 08/24/14 Pct Recovery = 62% Analysis Date = 08/24/14 Pct Recovery = 62% Analysis Date = 08/20/14 Pct Recovery = 62% Analysis Date = 08/20/14 Pct Recovery = 62% Analysis Date = 08/15/14 Pct Recovery = 61% Analysis Date = 08/15/14 Pct Recovery = 61% Analysis Date = 08/10/14 Pct Recovery = 61% Analysis Date = 08/10/14 Pct Recovery = 61% Analysis Date = 08/05/14 Pct Recovery = 61% Analysis Date = 08/05/14 Pct Recovery = 61% Analysis Date = 07/31/14 Pct Recovery = 61% Analysis Date = 07/31/14 Pct Recovery = 61% Analysis Date = 07/27/14 Pct Recovery = 61% Analysis Date = 07/27/14 Pct Recovery = 61% Analysis Date = 07/22/14 Pct Recovery = 61% Analysis Date = 07/22/14 Pct Recovery = 61% Analysis Date = 07/17/14 Pct Recovery = 61% Analysis Date = 07/17/14 Pct Recovery = 61% Analysis Date = 07/12/14 Pct Recovery = 61% Analysis Date = 07/12/14 Pct Recovery = 61% Analysis Date = 07/07/14 Pct Recovery = 61% Analysis Date = 07/07/14 Pct Recovery = 61% Analysis Date = 07/03/14 Pct Recovery = 61% Analysis Date = 07/03/14 Pct Recovery = 61% Analysis Date = 06/28/14 Pct Recovery = 61% Analysis Date = 06/28/14 Pct Recovery = 61% Analysis Date = 06/23/14 Pct Recovery = 61% Analysis Date = 06/23/14 Pct Recovery = 61% Analysis Date = 06/18/14 Pct Recovery = 61% Analysis Date = 06/18/14 Pct Recovery = 61% Analysis Date = 06/13/14 Pct Recovery = 61% Analysis Date = 06/13/14 Pct Recovery = 61% Analysis Date = 06/09/14 Pct Recovery = 61% Analysis Date = 06/09/14 Pct Recovery = 61% Analysis Date = 06/04/14 Pct Recovery = 60% Analysis Date = 06/04/14 Pct Recovery = 60% Analysis Date = 05/30/14 Pct Recovery = 60% Analysis Date = 05/30/14 Pct Recovery = 60% Analysis Date = 05/25/14 Pct Recovery = 60% Analysis Date = 05/25/14 Pct Recovery = 60% Analysis Date = 05/21/14 Pct Recovery = 60% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
DEXTROMETHORPHAN

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 2 50% 14% 50% 15%
>= Reporting Level 73 64% 12% 63% 13%
Total 75 63% 12% 62% 13%

Sample Statistics
DEXTROMETHORPHAN

Characteristic N % % Basis
Plotted 75 100% Spiked
Estimated Values 2 3% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 75 .  
False Negatives 0 0% 0 out of 75
Not Spiked 40 .  
False Positives 1 3% 1 out of 40

BQS OBSP Determination:
DIAZEPAM (VALIUM)
METHOD: 2440 , TESTIDCODE: 67499LCM56
Open Data Set

Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 89% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 83% Analysis Date = 01/17/16 SpikeMix = ERA 0406-15-09: 80 µl & ERA 0406-15-07A: 80 µl Pct Recovery = 68% Analysis Date = 11/24/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 81% Analysis Date = 10/01/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 119% Analysis Date = 11/04/15 SpikeMix = Abs 052215: 80 µl & Abs 050115: 80 µl Pct Recovery = 76% Analysis Date = 11/18/16 SpikeMix = ERA 04281604: 80 µl & ERA 04281603: 80 µl Pct Recovery = 96% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & ERA 04281604: 80 µl Pct Recovery = 85% Analysis Date = 09/24/16 SpikeMix = Crescent EN160610015: 80 µl & Abs 061416: 80 µl Pct Recovery = 73% Analysis Date = 09/24/16 SpikeMix = Abs 061416: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 65% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 86% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 83% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 88% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 87% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 50% Analysis Date = 12/07/14 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 60% Analysis Date = 10/25/14 SpikeMix = Abs 041614: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 81% Analysis Date = 06/22/14 SpikeMix = Abs 041814: 60 µl & Abs 041614: 60 µl Pct Recovery = 86% Analysis Date = 06/11/14 SpikeMix = Abs 041614: 60 µl & Abs 041714: 60 µl Pct Recovery = 61% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-08: 40 µl & ERA 0406-15-09: 40 µl Pct Recovery = 66% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-08: 40 µl & Abs 052215: 40 µl Pct Recovery = 57% Analysis Date = 02/23/16 SpikeMix = Abs 052215: 40 µl & Abs 050115: 40 µl Pct Recovery = 81% Analysis Date = 09/10/15 SpikeMix = Abs 052215: 40 µl & ERA 0406-15-07A: 40 µl Pct Recovery = 102% Analysis Date = 07/31/15 SpikeMix = Abs 051315: 40 µl & Abs 052215: 40 µl Pct Recovery = 65% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 91% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 119% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 62% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 74% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 97% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 105% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 65% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 57% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 70% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 79% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 63% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 55% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 68% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 58% Analysis Date = 04/30/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 52% Analysis Date = 02/10/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 71% Analysis Date = 10/24/14 SpikeMix = ERA 0319-14-05: 8 µl & Abs 041614: 8 µl Pct Recovery = 57% Analysis Date = 09/12/14 SpikeMix = Abs 041614: 30 µl & ERA 0319-14-04: 30 µl Pct Recovery = 57% Analysis Date = 07/13/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 37% Analysis Date = 06/28/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 81% Analysis Date = 05/30/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 48% Analysis Date = 05/17/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 78% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 46% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 103% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-08: 20 µl & ERA 0406-15-09: 20 µl Pct Recovery = 57% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-09: 20 µl Pct Recovery = 102% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 111% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 95% Analysis Date = 02/23/16 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 70% Analysis Date = 11/24/15 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 99% Analysis Date = 09/09/15 SpikeMix = ERA 0406-15-08: 20 µl & Abs 052215: 20 µl Pct Recovery = 101% Analysis Date = 06/26/15 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 70% Analysis Date = 01/04/17 Pct Recovery = 86% Analysis Date = 12/31/16 Pct Recovery = 86% Analysis Date = 12/31/16 Pct Recovery = 86% Analysis Date = 12/26/16 Pct Recovery = 86% Analysis Date = 12/26/16 Pct Recovery = 86% Analysis Date = 12/21/16 Pct Recovery = 85% Analysis Date = 12/21/16 Pct Recovery = 85% Analysis Date = 12/16/16 Pct Recovery = 85% Analysis Date = 12/16/16 Pct Recovery = 85% Analysis Date = 12/11/16 Pct Recovery = 85% Analysis Date = 12/11/16 Pct Recovery = 85% Analysis Date = 12/07/16 Pct Recovery = 84% Analysis Date = 12/07/16 Pct Recovery = 84% Analysis Date = 12/02/16 Pct Recovery = 84% Analysis Date = 12/02/16 Pct Recovery = 84% Analysis Date = 11/27/16 Pct Recovery = 84% Analysis Date = 11/27/16 Pct Recovery = 84% Analysis Date = 11/22/16 Pct Recovery = 83% Analysis Date = 11/22/16 Pct Recovery = 83% Analysis Date = 11/17/16 Pct Recovery = 83% Analysis Date = 11/17/16 Pct Recovery = 83% Analysis Date = 11/12/16 Pct Recovery = 83% Analysis Date = 11/12/16 Pct Recovery = 83% Analysis Date = 11/08/16 Pct Recovery = 82% Analysis Date = 11/08/16 Pct Recovery = 82% Analysis Date = 11/03/16 Pct Recovery = 82% Analysis Date = 11/03/16 Pct Recovery = 82% Analysis Date = 10/29/16 Pct Recovery = 82% Analysis Date = 10/29/16 Pct Recovery = 82% Analysis Date = 10/24/16 Pct Recovery = 82% Analysis Date = 10/24/16 Pct Recovery = 82% Analysis Date = 10/19/16 Pct Recovery = 81% Analysis Date = 10/19/16 Pct Recovery = 81% Analysis Date = 10/15/16 Pct Recovery = 81% Analysis Date = 10/15/16 Pct Recovery = 81% Analysis Date = 10/10/16 Pct Recovery = 81% Analysis Date = 10/10/16 Pct Recovery = 81% Analysis Date = 10/05/16 Pct Recovery = 80% Analysis Date = 10/05/16 Pct Recovery = 80% Analysis Date = 09/30/16 Pct Recovery = 80% Analysis Date = 09/30/16 Pct Recovery = 80% Analysis Date = 09/25/16 Pct Recovery = 80% Analysis Date = 09/25/16 Pct Recovery = 80% Analysis Date = 09/20/16 Pct Recovery = 80% Analysis Date = 09/20/16 Pct Recovery = 80% Analysis Date = 09/16/16 Pct Recovery = 80% Analysis Date = 09/16/16 Pct Recovery = 80% Analysis Date = 09/11/16 Pct Recovery = 79% Analysis Date = 09/11/16 Pct Recovery = 79% Analysis Date = 09/06/16 Pct Recovery = 79% Analysis Date = 09/06/16 Pct Recovery = 79% Analysis Date = 09/01/16 Pct Recovery = 79% Analysis Date = 09/01/16 Pct Recovery = 79% Analysis Date = 08/27/16 Pct Recovery = 79% Analysis Date = 08/27/16 Pct Recovery = 79% Analysis Date = 08/23/16 Pct Recovery = 79% Analysis Date = 08/23/16 Pct Recovery = 79% Analysis Date = 08/18/16 Pct Recovery = 78% Analysis Date = 08/18/16 Pct Recovery = 78% Analysis Date = 08/13/16 Pct Recovery = 78% Analysis Date = 08/13/16 Pct Recovery = 78% Analysis Date = 08/08/16 Pct Recovery = 78% Analysis Date = 08/08/16 Pct Recovery = 78% Analysis Date = 08/03/16 Pct Recovery = 78% Analysis Date = 08/03/16 Pct Recovery = 78% Analysis Date = 07/29/16 Pct Recovery = 78% Analysis Date = 07/29/16 Pct Recovery = 78% Analysis Date = 07/25/16 Pct Recovery = 77% Analysis Date = 07/25/16 Pct Recovery = 77% Analysis Date = 07/20/16 Pct Recovery = 77% Analysis Date = 07/20/16 Pct Recovery = 77% Analysis Date = 07/15/16 Pct Recovery = 77% Analysis Date = 07/15/16 Pct Recovery = 77% Analysis Date = 07/10/16 Pct Recovery = 77% Analysis Date = 07/10/16 Pct Recovery = 77% Analysis Date = 07/05/16 Pct Recovery = 77% Analysis Date = 07/05/16 Pct Recovery = 77% Analysis Date = 07/01/16 Pct Recovery = 77% Analysis Date = 07/01/16 Pct Recovery = 77% Analysis Date = 06/26/16 Pct Recovery = 77% Analysis Date = 06/26/16 Pct Recovery = 77% Analysis Date = 06/21/16 Pct Recovery = 77% Analysis Date = 06/21/16 Pct Recovery = 77% Analysis Date = 06/16/16 Pct Recovery = 77% Analysis Date = 06/16/16 Pct Recovery = 77% Analysis Date = 06/11/16 Pct Recovery = 77% Analysis Date = 06/11/16 Pct Recovery = 77% Analysis Date = 06/06/16 Pct Recovery = 77% Analysis Date = 06/06/16 Pct Recovery = 77% Analysis Date = 06/02/16 Pct Recovery = 77% Analysis Date = 06/02/16 Pct Recovery = 77% Analysis Date = 05/28/16 Pct Recovery = 77% Analysis Date = 05/28/16 Pct Recovery = 77% Analysis Date = 05/23/16 Pct Recovery = 77% Analysis Date = 05/23/16 Pct Recovery = 77% Analysis Date = 05/18/16 Pct Recovery = 77% Analysis Date = 05/18/16 Pct Recovery = 77% Analysis Date = 05/13/16 Pct Recovery = 77% Analysis Date = 05/13/16 Pct Recovery = 77% Analysis Date = 05/08/16 Pct Recovery = 77% Analysis Date = 05/08/16 Pct Recovery = 77% Analysis Date = 05/04/16 Pct Recovery = 77% Analysis Date = 05/04/16 Pct Recovery = 77% Analysis Date = 04/29/16 Pct Recovery = 77% Analysis Date = 04/29/16 Pct Recovery = 77% Analysis Date = 04/24/16 Pct Recovery = 77% Analysis Date = 04/24/16 Pct Recovery = 77% Analysis Date = 04/19/16 Pct Recovery = 77% Analysis Date = 04/19/16 Pct Recovery = 77% Analysis Date = 04/14/16 Pct Recovery = 78% Analysis Date = 04/14/16 Pct Recovery = 78% Analysis Date = 04/10/16 Pct Recovery = 78% Analysis Date = 04/10/16 Pct Recovery = 78% Analysis Date = 04/05/16 Pct Recovery = 78% Analysis Date = 04/05/16 Pct Recovery = 78% Analysis Date = 03/31/16 Pct Recovery = 78% Analysis Date = 03/31/16 Pct Recovery = 78% Analysis Date = 03/26/16 Pct Recovery = 79% Analysis Date = 03/26/16 Pct Recovery = 79% Analysis Date = 03/21/16 Pct Recovery = 79% Analysis Date = 03/21/16 Pct Recovery = 79% Analysis Date = 03/16/16 Pct Recovery = 79% Analysis Date = 03/16/16 Pct Recovery = 79% Analysis Date = 03/12/16 Pct Recovery = 79% Analysis Date = 03/12/16 Pct Recovery = 79% Analysis Date = 03/07/16 Pct Recovery = 79% Analysis Date = 03/07/16 Pct Recovery = 79% Analysis Date = 03/02/16 Pct Recovery = 80% Analysis Date = 03/02/16 Pct Recovery = 80% Analysis Date = 02/26/16 Pct Recovery = 80% Analysis Date = 02/26/16 Pct Recovery = 80% Analysis Date = 02/21/16 Pct Recovery = 80% Analysis Date = 02/21/16 Pct Recovery = 80% Analysis Date = 02/17/16 Pct Recovery = 80% Analysis Date = 02/17/16 Pct Recovery = 80% Analysis Date = 02/12/16 Pct Recovery = 81% Analysis Date = 02/12/16 Pct Recovery = 81% Analysis Date = 02/07/16 Pct Recovery = 81% Analysis Date = 02/07/16 Pct Recovery = 81% Analysis Date = 02/02/16 Pct Recovery = 81% Analysis Date = 02/02/16 Pct Recovery = 81% Analysis Date = 01/28/16 Pct Recovery = 81% Analysis Date = 01/28/16 Pct Recovery = 81% Analysis Date = 01/23/16 Pct Recovery = 82% Analysis Date = 01/23/16 Pct Recovery = 82% Analysis Date = 01/19/16 Pct Recovery = 82% Analysis Date = 01/19/16 Pct Recovery = 82% Analysis Date = 01/14/16 Pct Recovery = 82% Analysis Date = 01/14/16 Pct Recovery = 82% Analysis Date = 01/09/16 Pct Recovery = 82% Analysis Date = 01/09/16 Pct Recovery = 82% Analysis Date = 01/04/16 Pct Recovery = 82% Analysis Date = 01/04/16 Pct Recovery = 82% Analysis Date = 12/30/15 Pct Recovery = 82% Analysis Date = 12/30/15 Pct Recovery = 82% Analysis Date = 12/26/15 Pct Recovery = 82% Analysis Date = 12/26/15 Pct Recovery = 82% Analysis Date = 12/21/15 Pct Recovery = 82% Analysis Date = 12/21/15 Pct Recovery = 82% Analysis Date = 12/16/15 Pct Recovery = 81% Analysis Date = 12/16/15 Pct Recovery = 81% Analysis Date = 12/11/15 Pct Recovery = 81% Analysis Date = 12/11/15 Pct Recovery = 81% Analysis Date = 12/06/15 Pct Recovery = 81% Analysis Date = 12/06/15 Pct Recovery = 81% Analysis Date = 12/01/15 Pct Recovery = 81% Analysis Date = 12/01/15 Pct Recovery = 81% Analysis Date = 11/27/15 Pct Recovery = 81% Analysis Date = 11/27/15 Pct Recovery = 81% Analysis Date = 11/22/15 Pct Recovery = 81% Analysis Date = 11/22/15 Pct Recovery = 81% Analysis Date = 11/17/15 Pct Recovery = 81% Analysis Date = 11/17/15 Pct Recovery = 81% Analysis Date = 11/12/15 Pct Recovery = 81% Analysis Date = 11/12/15 Pct Recovery = 81% Analysis Date = 11/07/15 Pct Recovery = 81% Analysis Date = 11/07/15 Pct Recovery = 81% Analysis Date = 11/03/15 Pct Recovery = 81% Analysis Date = 11/03/15 Pct Recovery = 81% Analysis Date = 10/29/15 Pct Recovery = 81% Analysis Date = 10/29/15 Pct Recovery = 81% Analysis Date = 10/24/15 Pct Recovery = 80% Analysis Date = 10/24/15 Pct Recovery = 80% Analysis Date = 10/19/15 Pct Recovery = 80% Analysis Date = 10/19/15 Pct Recovery = 80% Analysis Date = 10/14/15 Pct Recovery = 80% Analysis Date = 10/14/15 Pct Recovery = 80% Analysis Date = 10/09/15 Pct Recovery = 80% Analysis Date = 10/09/15 Pct Recovery = 80% Analysis Date = 10/05/15 Pct Recovery = 79% Analysis Date = 10/05/15 Pct Recovery = 79% Analysis Date = 09/30/15 Pct Recovery = 79% Analysis Date = 09/30/15 Pct Recovery = 79% Analysis Date = 09/25/15 Pct Recovery = 79% Analysis Date = 09/25/15 Pct Recovery = 79% Analysis Date = 09/20/15 Pct Recovery = 79% Analysis Date = 09/20/15 Pct Recovery = 79% Analysis Date = 09/15/15 Pct Recovery = 78% Analysis Date = 09/15/15 Pct Recovery = 78% Analysis Date = 09/10/15 Pct Recovery = 78% Analysis Date = 09/10/15 Pct Recovery = 78% Analysis Date = 09/06/15 Pct Recovery = 78% Analysis Date = 09/06/15 Pct Recovery = 78% Analysis Date = 09/01/15 Pct Recovery = 78% Analysis Date = 09/01/15 Pct Recovery = 78% Analysis Date = 08/27/15 Pct Recovery = 78% Analysis Date = 08/27/15 Pct Recovery = 78% Analysis Date = 08/22/15 Pct Recovery = 77% Analysis Date = 08/22/15 Pct Recovery = 77% Analysis Date = 08/17/15 Pct Recovery = 77% Analysis Date = 08/17/15 Pct Recovery = 77% Analysis Date = 08/13/15 Pct Recovery = 77% Analysis Date = 08/13/15 Pct Recovery = 77% Analysis Date = 08/08/15 Pct Recovery = 77% Analysis Date = 08/08/15 Pct Recovery = 77% Analysis Date = 08/03/15 Pct Recovery = 76% Analysis Date = 08/03/15 Pct Recovery = 76% Analysis Date = 07/29/15 Pct Recovery = 76% Analysis Date = 07/29/15 Pct Recovery = 76% Analysis Date = 07/24/15 Pct Recovery = 76% Analysis Date = 07/24/15 Pct Recovery = 76% Analysis Date = 07/19/15 Pct Recovery = 76% Analysis Date = 07/19/15 Pct Recovery = 76% Analysis Date = 07/15/15 Pct Recovery = 75% Analysis Date = 07/15/15 Pct Recovery = 75% Analysis Date = 07/10/15 Pct Recovery = 75% Analysis Date = 07/10/15 Pct Recovery = 75% Analysis Date = 07/05/15 Pct Recovery = 75% Analysis Date = 07/05/15 Pct Recovery = 75% Analysis Date = 06/30/15 Pct Recovery = 75% Analysis Date = 06/30/15 Pct Recovery = 75% Analysis Date = 06/25/15 Pct Recovery = 74% Analysis Date = 06/25/15 Pct Recovery = 74% Analysis Date = 06/21/15 Pct Recovery = 74% Analysis Date = 06/21/15 Pct Recovery = 74% Analysis Date = 06/16/15 Pct Recovery = 74% Analysis Date = 06/16/15 Pct Recovery = 74% Analysis Date = 06/11/15 Pct Recovery = 74% Analysis Date = 06/11/15 Pct Recovery = 74% Analysis Date = 06/06/15 Pct Recovery = 74% Analysis Date = 06/06/15 Pct Recovery = 74% Analysis Date = 06/01/15 Pct Recovery = 74% Analysis Date = 06/01/15 Pct Recovery = 74% Analysis Date = 05/27/15 Pct Recovery = 74% Analysis Date = 05/27/15 Pct Recovery = 74% Analysis Date = 05/23/15 Pct Recovery = 73% Analysis Date = 05/23/15 Pct Recovery = 73% Analysis Date = 05/18/15 Pct Recovery = 73% Analysis Date = 05/18/15 Pct Recovery = 73% Analysis Date = 05/13/15 Pct Recovery = 73% Analysis Date = 05/13/15 Pct Recovery = 73% Analysis Date = 05/08/15 Pct Recovery = 73% Analysis Date = 05/08/15 Pct Recovery = 73% Analysis Date = 05/03/15 Pct Recovery = 73% Analysis Date = 05/03/15 Pct Recovery = 73% Analysis Date = 04/29/15 Pct Recovery = 73% Analysis Date = 04/29/15 Pct Recovery = 73% Analysis Date = 04/24/15 Pct Recovery = 73% Analysis Date = 04/24/15 Pct Recovery = 73% Analysis Date = 04/19/15 Pct Recovery = 72% Analysis Date = 04/19/15 Pct Recovery = 72% Analysis Date = 04/14/15 Pct Recovery = 72% Analysis Date = 04/14/15 Pct Recovery = 72% Analysis Date = 04/09/15 Pct Recovery = 72% Analysis Date = 04/09/15 Pct Recovery = 72% Analysis Date = 04/04/15 Pct Recovery = 72% Analysis Date = 04/04/15 Pct Recovery = 72% Analysis Date = 03/31/15 Pct Recovery = 72% Analysis Date = 03/31/15 Pct Recovery = 72% Analysis Date = 03/26/15 Pct Recovery = 72% Analysis Date = 03/26/15 Pct Recovery = 72% Analysis Date = 03/21/15 Pct Recovery = 72% Analysis Date = 03/21/15 Pct Recovery = 72% Analysis Date = 03/16/15 Pct Recovery = 71% Analysis Date = 03/16/15 Pct Recovery = 71% Analysis Date = 03/11/15 Pct Recovery = 71% Analysis Date = 03/11/15 Pct Recovery = 71% Analysis Date = 03/07/15 Pct Recovery = 71% Analysis Date = 03/07/15 Pct Recovery = 71% Analysis Date = 03/02/15 Pct Recovery = 71% Analysis Date = 03/02/15 Pct Recovery = 71% Analysis Date = 02/25/15 Pct Recovery = 71% Analysis Date = 02/25/15 Pct Recovery = 71% Analysis Date = 02/20/15 Pct Recovery = 71% Analysis Date = 02/20/15 Pct Recovery = 71% Analysis Date = 02/15/15 Pct Recovery = 71% Analysis Date = 02/15/15 Pct Recovery = 71% Analysis Date = 02/10/15 Pct Recovery = 70% Analysis Date = 02/10/15 Pct Recovery = 70% Analysis Date = 02/06/15 Pct Recovery = 70% Analysis Date = 02/06/15 Pct Recovery = 70% Analysis Date = 02/01/15 Pct Recovery = 70% Analysis Date = 02/01/15 Pct Recovery = 70% Analysis Date = 01/27/15 Pct Recovery = 70% Analysis Date = 01/27/15 Pct Recovery = 70% Analysis Date = 01/22/15 Pct Recovery = 70% Analysis Date = 01/22/15 Pct Recovery = 70% Analysis Date = 01/17/15 Pct Recovery = 70% Analysis Date = 01/17/15 Pct Recovery = 70% Analysis Date = 01/12/15 Pct Recovery = 69% Analysis Date = 01/12/15 Pct Recovery = 69% Analysis Date = 01/08/15 Pct Recovery = 69% Analysis Date = 01/08/15 Pct Recovery = 69% Analysis Date = 01/03/15 Pct Recovery = 69% Analysis Date = 01/03/15 Pct Recovery = 69% Analysis Date = 12/29/14 Pct Recovery = 69% Analysis Date = 12/29/14 Pct Recovery = 69% Analysis Date = 12/24/14 Pct Recovery = 69% Analysis Date = 12/24/14 Pct Recovery = 69% Analysis Date = 12/19/14 Pct Recovery = 68% Analysis Date = 12/19/14 Pct Recovery = 68% Analysis Date = 12/15/14 Pct Recovery = 68% Analysis Date = 12/15/14 Pct Recovery = 68% Analysis Date = 12/10/14 Pct Recovery = 68% Analysis Date = 12/10/14 Pct Recovery = 68% Analysis Date = 12/05/14 Pct Recovery = 68% Analysis Date = 12/05/14 Pct Recovery = 68% Analysis Date = 11/30/14 Pct Recovery = 68% Analysis Date = 11/30/14 Pct Recovery = 68% Analysis Date = 11/25/14 Pct Recovery = 68% Analysis Date = 11/25/14 Pct Recovery = 68% Analysis Date = 11/20/14 Pct Recovery = 67% Analysis Date = 11/20/14 Pct Recovery = 67% Analysis Date = 11/16/14 Pct Recovery = 67% Analysis Date = 11/16/14 Pct Recovery = 67% Analysis Date = 11/11/14 Pct Recovery = 67% Analysis Date = 11/11/14 Pct Recovery = 67% Analysis Date = 11/06/14 Pct Recovery = 67% Analysis Date = 11/06/14 Pct Recovery = 67% Analysis Date = 11/01/14 Pct Recovery = 67% Analysis Date = 11/01/14 Pct Recovery = 67% Analysis Date = 10/27/14 Pct Recovery = 67% Analysis Date = 10/27/14 Pct Recovery = 67% Analysis Date = 10/23/14 Pct Recovery = 66% Analysis Date = 10/23/14 Pct Recovery = 66% Analysis Date = 10/18/14 Pct Recovery = 66% Analysis Date = 10/18/14 Pct Recovery = 66% Analysis Date = 10/13/14 Pct Recovery = 66% Analysis Date = 10/13/14 Pct Recovery = 66% Analysis Date = 10/08/14 Pct Recovery = 66% Analysis Date = 10/08/14 Pct Recovery = 66% Analysis Date = 10/03/14 Pct Recovery = 66% Analysis Date = 10/03/14 Pct Recovery = 66% Analysis Date = 09/28/14 Pct Recovery = 66% Analysis Date = 09/28/14 Pct Recovery = 66% Analysis Date = 09/24/14 Pct Recovery = 65% Analysis Date = 09/24/14 Pct Recovery = 65% Analysis Date = 09/19/14 Pct Recovery = 65% Analysis Date = 09/19/14 Pct Recovery = 65% Analysis Date = 09/14/14 Pct Recovery = 65% Analysis Date = 09/14/14 Pct Recovery = 65% Analysis Date = 09/09/14 Pct Recovery = 65% Analysis Date = 09/09/14 Pct Recovery = 65% Analysis Date = 09/04/14 Pct Recovery = 65% Analysis Date = 09/04/14 Pct Recovery = 65% Analysis Date = 08/31/14 Pct Recovery = 65% Analysis Date = 08/31/14 Pct Recovery = 65% Analysis Date = 08/26/14 Pct Recovery = 64% Analysis Date = 08/26/14 Pct Recovery = 64% Analysis Date = 08/21/14 Pct Recovery = 64% Analysis Date = 08/21/14 Pct Recovery = 64% Analysis Date = 08/16/14 Pct Recovery = 64% Analysis Date = 08/16/14 Pct Recovery = 64% Analysis Date = 08/11/14 Pct Recovery = 64% Analysis Date = 08/11/14 Pct Recovery = 64% Analysis Date = 08/06/14 Pct Recovery = 64% Analysis Date = 08/06/14 Pct Recovery = 64% Analysis Date = 08/02/14 Pct Recovery = 64% Analysis Date = 08/02/14 Pct Recovery = 64% Analysis Date = 07/28/14 Pct Recovery = 63% Analysis Date = 07/28/14 Pct Recovery = 63% Analysis Date = 07/23/14 Pct Recovery = 63% Analysis Date = 07/23/14 Pct Recovery = 63% Analysis Date = 07/18/14 Pct Recovery = 63% Analysis Date = 07/18/14 Pct Recovery = 63% Analysis Date = 07/13/14 Pct Recovery = 63% Analysis Date = 07/13/14 Pct Recovery = 63% Analysis Date = 07/09/14 Pct Recovery = 63% Analysis Date = 07/09/14 Pct Recovery = 63% Analysis Date = 07/04/14 Pct Recovery = 63% Analysis Date = 07/04/14 Pct Recovery = 63% Analysis Date = 06/29/14 Pct Recovery = 62% Analysis Date = 06/29/14 Pct Recovery = 62% Analysis Date = 06/24/14 Pct Recovery = 62% Analysis Date = 06/24/14 Pct Recovery = 62% Analysis Date = 06/19/14 Pct Recovery = 62% Analysis Date = 06/19/14 Pct Recovery = 62% Analysis Date = 06/14/14 Pct Recovery = 62% Analysis Date = 06/14/14 Pct Recovery = 62% Analysis Date = 06/10/14 Pct Recovery = 62% Analysis Date = 06/10/14 Pct Recovery = 62% Analysis Date = 06/05/14 Pct Recovery = 62% Analysis Date = 06/05/14 Pct Recovery = 62% Analysis Date = 05/31/14 Pct Recovery = 61% Analysis Date = 05/31/14 Pct Recovery = 61% Analysis Date = 05/26/14 Pct Recovery = 61% Analysis Date = 05/26/14 Pct Recovery = 61% Analysis Date = 05/21/14 Pct Recovery = 61% Analysis Date = 05/21/14 Pct Recovery = 61% Analysis Date = 05/17/14 Pct Recovery = 61% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
DIAZEPAM (VALIUM)

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 56 76% 19% 75% 20%
Total 56 76% 19% 75% 20%

Sample Statistics
DIAZEPAM (VALIUM)

Characteristic N % % Basis
Plotted 56 89% Spiked
Estimated Values 3 5% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 3 5% Spiked
Spiked 63 .  
False Negatives 4 6% 4 out of 63
Not Spiked 52 .  
False Positives 0 0% 0 out of 52

BQS OBSP Determination:
DILTIAZEM
METHOD: 2440 , TESTIDCODE: 67519LCM56
Open Data Set

Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 84% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 76% Analysis Date = 01/17/16 SpikeMix = ERA 0406-15-09: 80 µl & ERA 0406-15-07A: 80 µl Pct Recovery = 69% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 80 µl & Abs 051315: 80 µl Pct Recovery = 58% Analysis Date = 11/18/16 SpikeMix = ERA 04281604: 80 µl & ERA 04281603: 80 µl Pct Recovery = 78% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & ERA 04281604: 80 µl Pct Recovery = 66% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 66% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 61% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 63% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 69% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 75% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 69% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 52% Analysis Date = 12/07/14 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 58% Analysis Date = 10/25/14 SpikeMix = Abs 041614: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 63% Analysis Date = 06/22/14 SpikeMix = Abs 041814: 60 µl & Abs 041614: 60 µl Pct Recovery = 64% Analysis Date = 06/11/14 SpikeMix = Abs 041614: 60 µl & Abs 041714: 60 µl Pct Recovery = 53% Analysis Date = 04/29/15 SpikeMix = ERA 0319-14-05: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 46% Analysis Date = 03/11/15 SpikeMix = ERA 0318-14-02: 15 µl & Abs 041714: 15 µl Pct Recovery = 61% Analysis Date = 02/06/15 SpikeMix = Abs 041814: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 54% Analysis Date = 12/06/14 SpikeMix = ERA 0318-14-02: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 44% Analysis Date = 10/11/14 SpikeMix = ERA 0318-14-02: 60 µl & ERA 0319-14-04: 60 µl Pct Recovery = 49% Analysis Date = 08/21/14 SpikeMix = ERA 0318-14-02: 60 µl & Abs 041714: 60 µl Pct Recovery = 42% Analysis Date = 07/26/14 SpikeMix = ERA 0319-14-05: 60 µl & ERA 0318-14-02: 60 µl Pct Recovery = 56% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-07A: 40 µl & Abs 051315: 40 µl Pct Recovery = 50% Analysis Date = 11/04/15 SpikeMix = ERA 0406-15-07A: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 59% Analysis Date = 09/10/15 SpikeMix = Abs 052215: 40 µl & ERA 0406-15-07A: 40 µl Pct Recovery = 50% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 60% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 63% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 64% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 78% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 83% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 98% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 72% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 71% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 64% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 65% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 66% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 92% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 59% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 49% Analysis Date = 04/30/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 29% Analysis Date = 02/10/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 40% Analysis Date = 10/24/14 SpikeMix = ERA 0319-14-05: 8 µl & Abs 041614: 8 µl Pct Recovery = 26% Analysis Date = 12/07/14 SpikeMix = ERA 0318-14-02: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 64% Analysis Date = 11/04/14 SpikeMix = Abs 041814: 8 µl & ERA 0318-14-02: 8 µl Pct Recovery = 51% Analysis Date = 07/13/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 36% Analysis Date = 06/28/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 39% Analysis Date = 05/30/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 53% Analysis Date = 05/17/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 52% Analysis Date = 10/10/14 SpikeMix = Abs 041814: 30 µl & ERA 0318-14-02: 30 µl Pct Recovery = 36% Analysis Date = 08/30/14 SpikeMix = ERA 0318-14-02: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 59% Analysis Date = 07/20/14 SpikeMix = ERA 0318-14-02: 30 µl & Abs 041714: 30 µl Pct Recovery = 44% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 54% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 50% Analysis Date = 04/27/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 77% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 52% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 64% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 55% Analysis Date = 11/24/15 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 59% Analysis Date = 09/15/15 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 61% Analysis Date = 01/18/17 Pct Recovery = 77% Analysis Date = 01/14/17 Pct Recovery = 77% Analysis Date = 01/14/17 Pct Recovery = 77% Analysis Date = 01/09/17 Pct Recovery = 76% Analysis Date = 01/09/17 Pct Recovery = 76% Analysis Date = 01/04/17 Pct Recovery = 76% Analysis Date = 01/04/17 Pct Recovery = 76% Analysis Date = 12/30/16 Pct Recovery = 76% Analysis Date = 12/30/16 Pct Recovery = 76% Analysis Date = 12/25/16 Pct Recovery = 75% Analysis Date = 12/25/16 Pct Recovery = 75% Analysis Date = 12/20/16 Pct Recovery = 75% Analysis Date = 12/20/16 Pct Recovery = 75% Analysis Date = 12/15/16 Pct Recovery = 75% Analysis Date = 12/15/16 Pct Recovery = 75% Analysis Date = 12/10/16 Pct Recovery = 74% Analysis Date = 12/10/16 Pct Recovery = 74% Analysis Date = 12/05/16 Pct Recovery = 74% Analysis Date = 12/05/16 Pct Recovery = 74% Analysis Date = 12/01/16 Pct Recovery = 74% Analysis Date = 12/01/16 Pct Recovery = 74% Analysis Date = 11/26/16 Pct Recovery = 73% Analysis Date = 11/26/16 Pct Recovery = 73% Analysis Date = 11/21/16 Pct Recovery = 73% Analysis Date = 11/21/16 Pct Recovery = 73% Analysis Date = 11/16/16 Pct Recovery = 73% Analysis Date = 11/16/16 Pct Recovery = 73% Analysis Date = 11/11/16 Pct Recovery = 72% Analysis Date = 11/11/16 Pct Recovery = 72% Analysis Date = 11/06/16 Pct Recovery = 72% Analysis Date = 11/06/16 Pct Recovery = 72% Analysis Date = 11/01/16 Pct Recovery = 72% Analysis Date = 11/01/16 Pct Recovery = 72% Analysis Date = 10/27/16 Pct Recovery = 71% Analysis Date = 10/27/16 Pct Recovery = 71% Analysis Date = 10/22/16 Pct Recovery = 71% Analysis Date = 10/22/16 Pct Recovery = 71% Analysis Date = 10/18/16 Pct Recovery = 71% Analysis Date = 10/18/16 Pct Recovery = 71% Analysis Date = 10/13/16 Pct Recovery = 70% Analysis Date = 10/13/16 Pct Recovery = 70% Analysis Date = 10/08/16 Pct Recovery = 70% Analysis Date = 10/08/16 Pct Recovery = 70% Analysis Date = 10/03/16 Pct Recovery = 70% Analysis Date = 10/03/16 Pct Recovery = 70% Analysis Date = 09/28/16 Pct Recovery = 70% Analysis Date = 09/28/16 Pct Recovery = 70% Analysis Date = 09/23/16 Pct Recovery = 69% Analysis Date = 09/23/16 Pct Recovery = 69% Analysis Date = 09/18/16 Pct Recovery = 69% Analysis Date = 09/18/16 Pct Recovery = 69% Analysis Date = 09/13/16 Pct Recovery = 69% Analysis Date = 09/13/16 Pct Recovery = 69% Analysis Date = 09/08/16 Pct Recovery = 68% Analysis Date = 09/08/16 Pct Recovery = 68% Analysis Date = 09/04/16 Pct Recovery = 68% Analysis Date = 09/04/16 Pct Recovery = 68% Analysis Date = 08/30/16 Pct Recovery = 68% Analysis Date = 08/30/16 Pct Recovery = 68% Analysis Date = 08/25/16 Pct Recovery = 67% Analysis Date = 08/25/16 Pct Recovery = 67% Analysis Date = 08/20/16 Pct Recovery = 67% Analysis Date = 08/20/16 Pct Recovery = 67% Analysis Date = 08/15/16 Pct Recovery = 67% Analysis Date = 08/15/16 Pct Recovery = 67% Analysis Date = 08/10/16 Pct Recovery = 67% Analysis Date = 08/10/16 Pct Recovery = 67% Analysis Date = 08/05/16 Pct Recovery = 66% Analysis Date = 08/05/16 Pct Recovery = 66% Analysis Date = 07/31/16 Pct Recovery = 66% Analysis Date = 07/31/16 Pct Recovery = 66% Analysis Date = 07/26/16 Pct Recovery = 66% Analysis Date = 07/26/16 Pct Recovery = 66% Analysis Date = 07/22/16 Pct Recovery = 65% Analysis Date = 07/22/16 Pct Recovery = 65% Analysis Date = 07/17/16 Pct Recovery = 65% Analysis Date = 07/17/16 Pct Recovery = 65% Analysis Date = 07/12/16 Pct Recovery = 65% Analysis Date = 07/12/16 Pct Recovery = 65% Analysis Date = 07/07/16 Pct Recovery = 65% Analysis Date = 07/07/16 Pct Recovery = 65% Analysis Date = 07/02/16 Pct Recovery = 65% Analysis Date = 07/02/16 Pct Recovery = 65% Analysis Date = 06/27/16 Pct Recovery = 64% Analysis Date = 06/27/16 Pct Recovery = 64% Analysis Date = 06/22/16 Pct Recovery = 64% Analysis Date = 06/22/16 Pct Recovery = 64% Analysis Date = 06/17/16 Pct Recovery = 64% Analysis Date = 06/17/16 Pct Recovery = 64% Analysis Date = 06/12/16 Pct Recovery = 64% Analysis Date = 06/12/16 Pct Recovery = 64% Analysis Date = 06/08/16 Pct Recovery = 64% Analysis Date = 06/08/16 Pct Recovery = 64% Analysis Date = 06/03/16 Pct Recovery = 64% Analysis Date = 06/03/16 Pct Recovery = 64% Analysis Date = 05/29/16 Pct Recovery = 63% Analysis Date = 05/29/16 Pct Recovery = 63% Analysis Date = 05/24/16 Pct Recovery = 63% Analysis Date = 05/24/16 Pct Recovery = 63% Analysis Date = 05/19/16 Pct Recovery = 63% Analysis Date = 05/19/16 Pct Recovery = 63% Analysis Date = 05/14/16 Pct Recovery = 63% Analysis Date = 05/14/16 Pct Recovery = 63% Analysis Date = 05/09/16 Pct Recovery = 63% Analysis Date = 05/09/16 Pct Recovery = 63% Analysis Date = 05/04/16 Pct Recovery = 62% Analysis Date = 05/04/16 Pct Recovery = 62% Analysis Date = 04/29/16 Pct Recovery = 62% Analysis Date = 04/29/16 Pct Recovery = 62% Analysis Date = 04/25/16 Pct Recovery = 62% Analysis Date = 04/25/16 Pct Recovery = 62% Analysis Date = 04/20/16 Pct Recovery = 62% Analysis Date = 04/20/16 Pct Recovery = 62% Analysis Date = 04/15/16 Pct Recovery = 62% Analysis Date = 04/15/16 Pct Recovery = 62% Analysis Date = 04/10/16 Pct Recovery = 62% Analysis Date = 04/10/16 Pct Recovery = 62% Analysis Date = 04/05/16 Pct Recovery = 61% Analysis Date = 04/05/16 Pct Recovery = 61% Analysis Date = 03/31/16 Pct Recovery = 61% Analysis Date = 03/31/16 Pct Recovery = 61% Analysis Date = 03/26/16 Pct Recovery = 61% Analysis Date = 03/26/16 Pct Recovery = 61% Analysis Date = 03/21/16 Pct Recovery = 61% Analysis Date = 03/21/16 Pct Recovery = 61% Analysis Date = 03/16/16 Pct Recovery = 61% Analysis Date = 03/16/16 Pct Recovery = 61% Analysis Date = 03/12/16 Pct Recovery = 61% Analysis Date = 03/12/16 Pct Recovery = 61% Analysis Date = 03/07/16 Pct Recovery = 60% Analysis Date = 03/07/16 Pct Recovery = 60% Analysis Date = 03/02/16 Pct Recovery = 60% Analysis Date = 03/02/16 Pct Recovery = 60% Analysis Date = 02/26/16 Pct Recovery = 60% Analysis Date = 02/26/16 Pct Recovery = 60% Analysis Date = 02/21/16 Pct Recovery = 60% Analysis Date = 02/21/16 Pct Recovery = 60% Analysis Date = 02/16/16 Pct Recovery = 60% Analysis Date = 02/16/16 Pct Recovery = 60% Analysis Date = 02/11/16 Pct Recovery = 60% Analysis Date = 02/11/16 Pct Recovery = 60% Analysis Date = 02/06/16 Pct Recovery = 60% Analysis Date = 02/06/16 Pct Recovery = 60% Analysis Date = 02/01/16 Pct Recovery = 59% Analysis Date = 02/01/16 Pct Recovery = 59% Analysis Date = 01/28/16 Pct Recovery = 59% Analysis Date = 01/28/16 Pct Recovery = 59% Analysis Date = 01/23/16 Pct Recovery = 59% Analysis Date = 01/23/16 Pct Recovery = 59% Analysis Date = 01/18/16 Pct Recovery = 59% Analysis Date = 01/18/16 Pct Recovery = 59% Analysis Date = 01/13/16 Pct Recovery = 59% Analysis Date = 01/13/16 Pct Recovery = 59% Analysis Date = 01/08/16 Pct Recovery = 59% Analysis Date = 01/08/16 Pct Recovery = 59% Analysis Date = 01/03/16 Pct Recovery = 59% Analysis Date = 01/03/16 Pct Recovery = 59% Analysis Date = 12/29/15 Pct Recovery = 58% Analysis Date = 12/29/15 Pct Recovery = 58% Analysis Date = 12/24/15 Pct Recovery = 58% Analysis Date = 12/24/15 Pct Recovery = 58% Analysis Date = 12/19/15 Pct Recovery = 58% Analysis Date = 12/19/15 Pct Recovery = 58% Analysis Date = 12/15/15 Pct Recovery = 58% Analysis Date = 12/15/15 Pct Recovery = 58% Analysis Date = 12/10/15 Pct Recovery = 58% Analysis Date = 12/10/15 Pct Recovery = 58% Analysis Date = 12/05/15 Pct Recovery = 58% Analysis Date = 12/05/15 Pct Recovery = 58% Analysis Date = 11/30/15 Pct Recovery = 58% Analysis Date = 11/30/15 Pct Recovery = 58% Analysis Date = 11/25/15 Pct Recovery = 57% Analysis Date = 11/25/15 Pct Recovery = 57% Analysis Date = 11/20/15 Pct Recovery = 57% Analysis Date = 11/20/15 Pct Recovery = 57% Analysis Date = 11/15/15 Pct Recovery = 57% Analysis Date = 11/15/15 Pct Recovery = 57% Analysis Date = 11/10/15 Pct Recovery = 57% Analysis Date = 11/10/15 Pct Recovery = 57% Analysis Date = 11/05/15 Pct Recovery = 57% Analysis Date = 11/05/15 Pct Recovery = 57% Analysis Date = 11/01/15 Pct Recovery = 57% Analysis Date = 11/01/15 Pct Recovery = 57% Analysis Date = 10/27/15 Pct Recovery = 57% Analysis Date = 10/27/15 Pct Recovery = 57% Analysis Date = 10/22/15 Pct Recovery = 56% Analysis Date = 10/22/15 Pct Recovery = 56% Analysis Date = 10/17/15 Pct Recovery = 56% Analysis Date = 10/17/15 Pct Recovery = 56% Analysis Date = 10/12/15 Pct Recovery = 56% Analysis Date = 10/12/15 Pct Recovery = 56% Analysis Date = 10/07/15 Pct Recovery = 56% Analysis Date = 10/07/15 Pct Recovery = 56% Analysis Date = 10/02/15 Pct Recovery = 56% Analysis Date = 10/02/15 Pct Recovery = 56% Analysis Date = 09/27/15 Pct Recovery = 56% Analysis Date = 09/27/15 Pct Recovery = 56% Analysis Date = 09/22/15 Pct Recovery = 56% Analysis Date = 09/22/15 Pct Recovery = 56% Analysis Date = 09/17/15 Pct Recovery = 56% Analysis Date = 09/17/15 Pct Recovery = 56% Analysis Date = 09/13/15 Pct Recovery = 55% Analysis Date = 09/13/15 Pct Recovery = 55% Analysis Date = 09/08/15 Pct Recovery = 55% Analysis Date = 09/08/15 Pct Recovery = 55% Analysis Date = 09/03/15 Pct Recovery = 55% Analysis Date = 09/03/15 Pct Recovery = 55% Analysis Date = 08/29/15 Pct Recovery = 55% Analysis Date = 08/29/15 Pct Recovery = 55% Analysis Date = 08/24/15 Pct Recovery = 55% Analysis Date = 08/24/15 Pct Recovery = 55% Analysis Date = 08/19/15 Pct Recovery = 55% Analysis Date = 08/19/15 Pct Recovery = 55% Analysis Date = 08/14/15 Pct Recovery = 55% Analysis Date = 08/14/15 Pct Recovery = 55% Analysis Date = 08/09/15 Pct Recovery = 54% Analysis Date = 08/09/15 Pct Recovery = 54% Analysis Date = 08/04/15 Pct Recovery = 54% Analysis Date = 08/04/15 Pct Recovery = 54% Analysis Date = 07/31/15 Pct Recovery = 54% Analysis Date = 07/31/15 Pct Recovery = 54% Analysis Date = 07/26/15 Pct Recovery = 54% Analysis Date = 07/26/15 Pct Recovery = 54% Analysis Date = 07/21/15 Pct Recovery = 54% Analysis Date = 07/21/15 Pct Recovery = 54% Analysis Date = 07/16/15 Pct Recovery = 54% Analysis Date = 07/16/15 Pct Recovery = 54% Analysis Date = 07/11/15 Pct Recovery = 54% Analysis Date = 07/11/15 Pct Recovery = 54% Analysis Date = 07/06/15 Pct Recovery = 54% Analysis Date = 07/06/15 Pct Recovery = 54% Analysis Date = 07/01/15 Pct Recovery = 53% Analysis Date = 07/01/15 Pct Recovery = 53% Analysis Date = 06/26/15 Pct Recovery = 53% Analysis Date = 06/26/15 Pct Recovery = 53% Analysis Date = 06/21/15 Pct Recovery = 53% Analysis Date = 06/21/15 Pct Recovery = 53% Analysis Date = 06/17/15 Pct Recovery = 53% Analysis Date = 06/17/15 Pct Recovery = 53% Analysis Date = 06/12/15 Pct Recovery = 53% Analysis Date = 06/12/15 Pct Recovery = 53% Analysis Date = 06/07/15 Pct Recovery = 53% Analysis Date = 06/07/15 Pct Recovery = 53% Analysis Date = 06/02/15 Pct Recovery = 53% Analysis Date = 06/02/15 Pct Recovery = 53% Analysis Date = 05/28/15 Pct Recovery = 52% Analysis Date = 05/28/15 Pct Recovery = 52% Analysis Date = 05/23/15 Pct Recovery = 52% Analysis Date = 05/23/15 Pct Recovery = 52% Analysis Date = 05/18/15 Pct Recovery = 52% Analysis Date = 05/18/15 Pct Recovery = 52% Analysis Date = 05/13/15 Pct Recovery = 52% Analysis Date = 05/13/15 Pct Recovery = 52% Analysis Date = 05/08/15 Pct Recovery = 52% Analysis Date = 05/08/15 Pct Recovery = 52% Analysis Date = 05/04/15 Pct Recovery = 52% Analysis Date = 05/04/15 Pct Recovery = 52% Analysis Date = 04/29/15 Pct Recovery = 52% Analysis Date = 04/29/15 Pct Recovery = 52% Analysis Date = 04/24/15 Pct Recovery = 52% Analysis Date = 04/24/15 Pct Recovery = 52% Analysis Date = 04/19/15 Pct Recovery = 51% Analysis Date = 04/19/15 Pct Recovery = 51% Analysis Date = 04/14/15 Pct Recovery = 51% Analysis Date = 04/14/15 Pct Recovery = 51% Analysis Date = 04/09/15 Pct Recovery = 51% Analysis Date = 04/09/15 Pct Recovery = 51% Analysis Date = 04/04/15 Pct Recovery = 51% Analysis Date = 04/04/15 Pct Recovery = 51% Analysis Date = 03/30/15 Pct Recovery = 51% Analysis Date = 03/30/15 Pct Recovery = 51% Analysis Date = 03/25/15 Pct Recovery = 51% Analysis Date = 03/25/15 Pct Recovery = 51% Analysis Date = 03/21/15 Pct Recovery = 51% Analysis Date = 03/21/15 Pct Recovery = 51% Analysis Date = 03/16/15 Pct Recovery = 51% Analysis Date = 03/16/15 Pct Recovery = 51% Analysis Date = 03/11/15 Pct Recovery = 51% Analysis Date = 03/11/15 Pct Recovery = 51% Analysis Date = 03/06/15 Pct Recovery = 51% Analysis Date = 03/06/15 Pct Recovery = 51% Analysis Date = 03/01/15 Pct Recovery = 51% Analysis Date = 03/01/15 Pct Recovery = 51% Analysis Date = 02/24/15 Pct Recovery = 51% Analysis Date = 02/24/15 Pct Recovery = 51% Analysis Date = 02/19/15 Pct Recovery = 51% Analysis Date = 02/19/15 Pct Recovery = 51% Analysis Date = 02/14/15 Pct Recovery = 51% Analysis Date = 02/14/15 Pct Recovery = 51% Analysis Date = 02/09/15 Pct Recovery = 50% Analysis Date = 02/09/15 Pct Recovery = 50% Analysis Date = 02/05/15 Pct Recovery = 50% Analysis Date = 02/05/15 Pct Recovery = 50% Analysis Date = 01/31/15 Pct Recovery = 50% Analysis Date = 01/31/15 Pct Recovery = 50% Analysis Date = 01/26/15 Pct Recovery = 50% Analysis Date = 01/26/15 Pct Recovery = 50% Analysis Date = 01/21/15 Pct Recovery = 50% Analysis Date = 01/21/15 Pct Recovery = 50% Analysis Date = 01/16/15 Pct Recovery = 50% Analysis Date = 01/16/15 Pct Recovery = 50% Analysis Date = 01/11/15 Pct Recovery = 50% Analysis Date = 01/11/15 Pct Recovery = 50% Analysis Date = 01/06/15 Pct Recovery = 50% Analysis Date = 01/06/15 Pct Recovery = 50% Analysis Date = 01/01/15 Pct Recovery = 50% Analysis Date = 01/01/15 Pct Recovery = 50% Analysis Date = 12/27/14 Pct Recovery = 50% Analysis Date = 12/27/14 Pct Recovery = 50% Analysis Date = 12/23/14 Pct Recovery = 50% Analysis Date = 12/23/14 Pct Recovery = 50% Analysis Date = 12/18/14 Pct Recovery = 50% Analysis Date = 12/18/14 Pct Recovery = 50% Analysis Date = 12/13/14 Pct Recovery = 50% Analysis Date = 12/13/14 Pct Recovery = 50% Analysis Date = 12/08/14 Pct Recovery = 50% Analysis Date = 12/08/14 Pct Recovery = 50% Analysis Date = 12/03/14 Pct Recovery = 50% Analysis Date = 12/03/14 Pct Recovery = 50% Analysis Date = 11/28/14 Pct Recovery = 50% Analysis Date = 11/28/14 Pct Recovery = 50% Analysis Date = 11/23/14 Pct Recovery = 50% Analysis Date = 11/23/14 Pct Recovery = 50% Analysis Date = 11/18/14 Pct Recovery = 50% Analysis Date = 11/18/14 Pct Recovery = 50% Analysis Date = 11/13/14 Pct Recovery = 50% Analysis Date = 11/13/14 Pct Recovery = 50% Analysis Date = 11/09/14 Pct Recovery = 50% Analysis Date = 11/09/14 Pct Recovery = 50% Analysis Date = 11/04/14 Pct Recovery = 50% Analysis Date = 11/04/14 Pct Recovery = 50% Analysis Date = 10/30/14 Pct Recovery = 50% Analysis Date = 10/30/14 Pct Recovery = 50% Analysis Date = 10/25/14 Pct Recovery = 49% Analysis Date = 10/25/14 Pct Recovery = 49% Analysis Date = 10/20/14 Pct Recovery = 49% Analysis Date = 10/20/14 Pct Recovery = 49% Analysis Date = 10/15/14 Pct Recovery = 49% Analysis Date = 10/15/14 Pct Recovery = 49% Analysis Date = 10/10/14 Pct Recovery = 49% Analysis Date = 10/10/14 Pct Recovery = 49% Analysis Date = 10/05/14 Pct Recovery = 49% Analysis Date = 10/05/14 Pct Recovery = 49% Analysis Date = 09/30/14 Pct Recovery = 49% Analysis Date = 09/30/14 Pct Recovery = 49% Analysis Date = 09/26/14 Pct Recovery = 49% Analysis Date = 09/26/14 Pct Recovery = 49% Analysis Date = 09/21/14 Pct Recovery = 49% Analysis Date = 09/21/14 Pct Recovery = 49% Analysis Date = 09/16/14 Pct Recovery = 49% Analysis Date = 09/16/14 Pct Recovery = 49% Analysis Date = 09/11/14 Pct Recovery = 49% Analysis Date = 09/11/14 Pct Recovery = 49% Analysis Date = 09/06/14 Pct Recovery = 49% Analysis Date = 09/06/14 Pct Recovery = 49% Analysis Date = 09/01/14 Pct Recovery = 49% Analysis Date = 09/01/14 Pct Recovery = 49% Analysis Date = 08/27/14 Pct Recovery = 49% Analysis Date = 08/27/14 Pct Recovery = 49% Analysis Date = 08/22/14 Pct Recovery = 49% Analysis Date = 08/22/14 Pct Recovery = 49% Analysis Date = 08/17/14 Pct Recovery = 49% Analysis Date = 08/17/14 Pct Recovery = 49% Analysis Date = 08/13/14 Pct Recovery = 49% Analysis Date = 08/13/14 Pct Recovery = 49% Analysis Date = 08/08/14 Pct Recovery = 49% Analysis Date = 08/08/14 Pct Recovery = 49% Analysis Date = 08/03/14 Pct Recovery = 49% Analysis Date = 08/03/14 Pct Recovery = 49% Analysis Date = 07/29/14 Pct Recovery = 49% Analysis Date = 07/29/14 Pct Recovery = 49% Analysis Date = 07/24/14 Pct Recovery = 49% Analysis Date = 07/24/14 Pct Recovery = 49% Analysis Date = 07/19/14 Pct Recovery = 49% Analysis Date = 07/19/14 Pct Recovery = 49% Analysis Date = 07/14/14 Pct Recovery = 49% Analysis Date = 07/14/14 Pct Recovery = 49% Analysis Date = 07/09/14 Pct Recovery = 49% Analysis Date = 07/09/14 Pct Recovery = 49% Analysis Date = 07/04/14 Pct Recovery = 49% Analysis Date = 07/04/14 Pct Recovery = 49% Analysis Date = 06/30/14 Pct Recovery = 49% Analysis Date = 06/30/14 Pct Recovery = 49% Analysis Date = 06/25/14 Pct Recovery = 49% Analysis Date = 06/25/14 Pct Recovery = 49% Analysis Date = 06/20/14 Pct Recovery = 49% Analysis Date = 06/20/14 Pct Recovery = 49% Analysis Date = 06/15/14 Pct Recovery = 49% Analysis Date = 06/15/14 Pct Recovery = 49% Analysis Date = 06/10/14 Pct Recovery = 49% Analysis Date = 06/10/14 Pct Recovery = 49% Analysis Date = 06/05/14 Pct Recovery = 49% Analysis Date = 06/05/14 Pct Recovery = 49% Analysis Date = 05/31/14 Pct Recovery = 49% Analysis Date = 05/31/14 Pct Recovery = 49% Analysis Date = 05/26/14 Pct Recovery = 49% Analysis Date = 05/26/14 Pct Recovery = 49% Analysis Date = 05/21/14 Pct Recovery = 49% Analysis Date = 05/21/14 Pct Recovery = 49% Analysis Date = 05/17/14 Pct Recovery = 49% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
DILTIAZEM

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 61 59% 14% 59% 11%
Total 61 59% 14% 59% 11%

Sample Statistics
DILTIAZEM

Characteristic N % % Basis
Plotted 61 97% Spiked
Estimated Values 4 6% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 63 .  
False Negatives 2 3% 2 out of 63
Not Spiked 38 .  
False Positives 0 0% 0 out of 38

BQS OBSP Determination:
DIPHENHYDRAMINE
METHOD: 2440 , TESTIDCODE: 67447LCM56
Open Data Set

Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 70% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 76% Analysis Date = 01/17/16 SpikeMix = ERA 0406-15-09: 80 µl & ERA 0406-15-07A: 80 µl Pct Recovery = 69% Analysis Date = 11/24/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 75% Analysis Date = 10/01/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 61% Analysis Date = 11/05/15 SpikeMix = ERA 0406-15-08: 80 µl & Abs 052215: 80 µl Pct Recovery = 71% Analysis Date = 11/04/15 SpikeMix = Abs 052215: 80 µl & Abs 050115: 80 µl Pct Recovery = 80% Analysis Date = 11/18/16 SpikeMix = ERA 04281604: 80 µl & ERA 04281603: 80 µl Pct Recovery = 81% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & ERA 04281604: 80 µl Pct Recovery = 76% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 64% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 66% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 73% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 78% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 83% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 81% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-04: 15 µl & Abs 041814: 15 µl Pct Recovery = 68% Analysis Date = 12/06/14 SpikeMix = ERA 0318-14-02: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 71% Analysis Date = 10/25/14 SpikeMix = Abs 041614: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 77% Analysis Date = 10/11/14 SpikeMix = ERA 0318-14-02: 60 µl & ERA 0319-14-04: 60 µl Pct Recovery = 65% Analysis Date = 08/28/14 SpikeMix = ERA 0319-14-04: 60 µl & ERA 0319-14-05: 60 µl Pct Recovery = 58% Analysis Date = 05/07/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 92% Analysis Date = 03/11/15 SpikeMix = ERA 0318-14-02: 15 µl & Abs 041714: 15 µl Pct Recovery = 78% Analysis Date = 01/16/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 74% Analysis Date = 12/06/14 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 67% Analysis Date = 08/21/14 SpikeMix = ERA 0318-14-02: 60 µl & Abs 041714: 60 µl Pct Recovery = 58% Analysis Date = 07/12/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 67% Analysis Date = 06/11/14 SpikeMix = Abs 041614: 60 µl & Abs 041714: 60 µl Pct Recovery = 65% Analysis Date = 05/21/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 67% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-08: 40 µl & ERA 0406-15-09: 40 µl Pct Recovery = 79% Analysis Date = 07/31/15 SpikeMix = ERA 0406-15-09: 40 µl & Abs 050115: 40 µl Pct Recovery = 58% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-08: 40 µl & Abs 052215: 40 µl Pct Recovery = 64% Analysis Date = 02/23/16 SpikeMix = Abs 052215: 40 µl & Abs 050115: 40 µl Pct Recovery = 67% Analysis Date = 07/31/15 SpikeMix = Abs 051315: 40 µl & Abs 052215: 40 µl Pct Recovery = 90% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 60% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 65% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 74% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 77% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 82% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 95% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 65% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 57% Analysis Date = 04/30/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 72% Analysis Date = 04/10/15 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 67% Analysis Date = 02/10/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 62% Analysis Date = 12/07/14 SpikeMix = ERA 0318-14-02: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 78% Analysis Date = 10/11/14 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 63% Analysis Date = 11/04/14 SpikeMix = Abs 041714: 8 µl & ERA 0319-14-05: 8 µl Pct Recovery = 63% Analysis Date = 09/12/14 SpikeMix = Abs 041614: 30 µl & ERA 0319-14-04: 30 µl Pct Recovery = 55% Analysis Date = 08/16/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 61% Analysis Date = 07/13/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 54% Analysis Date = 10/10/14 SpikeMix = Abs 041714: 30 µl & Abs 041814: 30 µl Pct Recovery = 69% Analysis Date = 07/20/14 SpikeMix = ERA 0318-14-02: 30 µl & Abs 041714: 30 µl Pct Recovery = 55% Analysis Date = 06/28/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 53% Analysis Date = 05/17/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 66% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 72% Analysis Date = 11/24/15 SpikeMix = ERA 0406-15-09: 20 µl & Abs 050115: 20 µl Pct Recovery = 79% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 63% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 66% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 117% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 140% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 83% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 80% Analysis Date = 01/18/17 Pct Recovery = 82% Analysis Date = 01/14/17 Pct Recovery = 82% Analysis Date = 01/14/17 Pct Recovery = 82% Analysis Date = 01/09/17 Pct Recovery = 82% Analysis Date = 01/09/17 Pct Recovery = 82% Analysis Date = 01/04/17 Pct Recovery = 82% Analysis Date = 01/04/17 Pct Recovery = 82% Analysis Date = 12/30/16 Pct Recovery = 82% Analysis Date = 12/30/16 Pct Recovery = 82% Analysis Date = 12/25/16 Pct Recovery = 81% Analysis Date = 12/25/16 Pct Recovery = 81% Analysis Date = 12/20/16 Pct Recovery = 81% Analysis Date = 12/20/16 Pct Recovery = 81% Analysis Date = 12/15/16 Pct Recovery = 81% Analysis Date = 12/15/16 Pct Recovery = 81% Analysis Date = 12/10/16 Pct Recovery = 81% Analysis Date = 12/10/16 Pct Recovery = 81% Analysis Date = 12/05/16 Pct Recovery = 81% Analysis Date = 12/05/16 Pct Recovery = 81% Analysis Date = 12/01/16 Pct Recovery = 80% Analysis Date = 12/01/16 Pct Recovery = 80% Analysis Date = 11/26/16 Pct Recovery = 80% Analysis Date = 11/26/16 Pct Recovery = 80% Analysis Date = 11/21/16 Pct Recovery = 80% Analysis Date = 11/21/16 Pct Recovery = 80% Analysis Date = 11/16/16 Pct Recovery = 80% Analysis Date = 11/16/16 Pct Recovery = 80% Analysis Date = 11/11/16 Pct Recovery = 80% Analysis Date = 11/11/16 Pct Recovery = 80% Analysis Date = 11/06/16 Pct Recovery = 79% Analysis Date = 11/06/16 Pct Recovery = 79% Analysis Date = 11/01/16 Pct Recovery = 79% Analysis Date = 11/01/16 Pct Recovery = 79% Analysis Date = 10/27/16 Pct Recovery = 79% Analysis Date = 10/27/16 Pct Recovery = 79% Analysis Date = 10/22/16 Pct Recovery = 79% Analysis Date = 10/22/16 Pct Recovery = 79% Analysis Date = 10/18/16 Pct Recovery = 79% Analysis Date = 10/18/16 Pct Recovery = 79% Analysis Date = 10/13/16 Pct Recovery = 78% Analysis Date = 10/13/16 Pct Recovery = 78% Analysis Date = 10/08/16 Pct Recovery = 78% Analysis Date = 10/08/16 Pct Recovery = 78% Analysis Date = 10/03/16 Pct Recovery = 78% Analysis Date = 10/03/16 Pct Recovery = 78% Analysis Date = 09/28/16 Pct Recovery = 78% Analysis Date = 09/28/16 Pct Recovery = 78% Analysis Date = 09/23/16 Pct Recovery = 78% Analysis Date = 09/23/16 Pct Recovery = 78% Analysis Date = 09/18/16 Pct Recovery = 78% Analysis Date = 09/18/16 Pct Recovery = 78% Analysis Date = 09/13/16 Pct Recovery = 77% Analysis Date = 09/13/16 Pct Recovery = 77% Analysis Date = 09/08/16 Pct Recovery = 77% Analysis Date = 09/08/16 Pct Recovery = 77% Analysis Date = 09/04/16 Pct Recovery = 77% Analysis Date = 09/04/16 Pct Recovery = 77% Analysis Date = 08/30/16 Pct Recovery = 77% Analysis Date = 08/30/16 Pct Recovery = 77% Analysis Date = 08/25/16 Pct Recovery = 77% Analysis Date = 08/25/16 Pct Recovery = 77% Analysis Date = 08/20/16 Pct Recovery = 77% Analysis Date = 08/20/16 Pct Recovery = 77% Analysis Date = 08/15/16 Pct Recovery = 76% Analysis Date = 08/15/16 Pct Recovery = 76% Analysis Date = 08/10/16 Pct Recovery = 76% Analysis Date = 08/10/16 Pct Recovery = 76% Analysis Date = 08/05/16 Pct Recovery = 76% Analysis Date = 08/05/16 Pct Recovery = 76% Analysis Date = 07/31/16 Pct Recovery = 76% Analysis Date = 07/31/16 Pct Recovery = 76% Analysis Date = 07/26/16 Pct Recovery = 76% Analysis Date = 07/26/16 Pct Recovery = 76% Analysis Date = 07/22/16 Pct Recovery = 76% Analysis Date = 07/22/16 Pct Recovery = 76% Analysis Date = 07/17/16 Pct Recovery = 76% Analysis Date = 07/17/16 Pct Recovery = 76% Analysis Date = 07/12/16 Pct Recovery = 75% Analysis Date = 07/12/16 Pct Recovery = 75% Analysis Date = 07/07/16 Pct Recovery = 75% Analysis Date = 07/07/16 Pct Recovery = 75% Analysis Date = 07/02/16 Pct Recovery = 75% Analysis Date = 07/02/16 Pct Recovery = 75% Analysis Date = 06/27/16 Pct Recovery = 75% Analysis Date = 06/27/16 Pct Recovery = 75% Analysis Date = 06/22/16 Pct Recovery = 75% Analysis Date = 06/22/16 Pct Recovery = 75% Analysis Date = 06/17/16 Pct Recovery = 75% Analysis Date = 06/17/16 Pct Recovery = 75% Analysis Date = 06/12/16 Pct Recovery = 75% Analysis Date = 06/12/16 Pct Recovery = 75% Analysis Date = 06/08/16 Pct Recovery = 75% Analysis Date = 06/08/16 Pct Recovery = 75% Analysis Date = 06/03/16 Pct Recovery = 75% Analysis Date = 06/03/16 Pct Recovery = 75% Analysis Date = 05/29/16 Pct Recovery = 75% Analysis Date = 05/29/16 Pct Recovery = 75% Analysis Date = 05/24/16 Pct Recovery = 75% Analysis Date = 05/24/16 Pct Recovery = 75% Analysis Date = 05/19/16 Pct Recovery = 75% Analysis Date = 05/19/16 Pct Recovery = 75% Analysis Date = 05/14/16 Pct Recovery = 75% Analysis Date = 05/14/16 Pct Recovery = 75% Analysis Date = 05/09/16 Pct Recovery = 75% Analysis Date = 05/09/16 Pct Recovery = 75% Analysis Date = 05/04/16 Pct Recovery = 75% Analysis Date = 05/04/16 Pct Recovery = 75% Analysis Date = 04/29/16 Pct Recovery = 74% Analysis Date = 04/29/16 Pct Recovery = 74% Analysis Date = 04/25/16 Pct Recovery = 74% Analysis Date = 04/25/16 Pct Recovery = 74% Analysis Date = 04/20/16 Pct Recovery = 74% Analysis Date = 04/20/16 Pct Recovery = 74% Analysis Date = 04/15/16 Pct Recovery = 74% Analysis Date = 04/15/16 Pct Recovery = 74% Analysis Date = 04/10/16 Pct Recovery = 74% Analysis Date = 04/10/16 Pct Recovery = 74% Analysis Date = 04/05/16 Pct Recovery = 74% Analysis Date = 04/05/16 Pct Recovery = 74% Analysis Date = 03/31/16 Pct Recovery = 74% Analysis Date = 03/31/16 Pct Recovery = 74% Analysis Date = 03/26/16 Pct Recovery = 74% Analysis Date = 03/26/16 Pct Recovery = 74% Analysis Date = 03/21/16 Pct Recovery = 74% Analysis Date = 03/21/16 Pct Recovery = 74% Analysis Date = 03/16/16 Pct Recovery = 74% Analysis Date = 03/16/16 Pct Recovery = 74% Analysis Date = 03/12/16 Pct Recovery = 74% Analysis Date = 03/12/16 Pct Recovery = 74% Analysis Date = 03/07/16 Pct Recovery = 74% Analysis Date = 03/07/16 Pct Recovery = 74% Analysis Date = 03/02/16 Pct Recovery = 74% Analysis Date = 03/02/16 Pct Recovery = 74% Analysis Date = 02/26/16 Pct Recovery = 74% Analysis Date = 02/26/16 Pct Recovery = 74% Analysis Date = 02/21/16 Pct Recovery = 73% Analysis Date = 02/21/16 Pct Recovery = 73% Analysis Date = 02/16/16 Pct Recovery = 73% Analysis Date = 02/16/16 Pct Recovery = 73% Analysis Date = 02/11/16 Pct Recovery = 73% Analysis Date = 02/11/16 Pct Recovery = 73% Analysis Date = 02/06/16 Pct Recovery = 73% Analysis Date = 02/06/16 Pct Recovery = 73% Analysis Date = 02/01/16 Pct Recovery = 73% Analysis Date = 02/01/16 Pct Recovery = 73% Analysis Date = 01/28/16 Pct Recovery = 73% Analysis Date = 01/28/16 Pct Recovery = 73% Analysis Date = 01/23/16 Pct Recovery = 73% Analysis Date = 01/23/16 Pct Recovery = 73% Analysis Date = 01/18/16 Pct Recovery = 73% Analysis Date = 01/18/16 Pct Recovery = 73% Analysis Date = 01/13/16 Pct Recovery = 73% Analysis Date = 01/13/16 Pct Recovery = 73% Analysis Date = 01/08/16 Pct Recovery = 73% Analysis Date = 01/08/16 Pct Recovery = 73% Analysis Date = 01/03/16 Pct Recovery = 73% Analysis Date = 01/03/16 Pct Recovery = 73% Analysis Date = 12/29/15 Pct Recovery = 73% Analysis Date = 12/29/15 Pct Recovery = 73% Analysis Date = 12/24/15 Pct Recovery = 73% Analysis Date = 12/24/15 Pct Recovery = 73% Analysis Date = 12/19/15 Pct Recovery = 73% Analysis Date = 12/19/15 Pct Recovery = 73% Analysis Date = 12/15/15 Pct Recovery = 73% Analysis Date = 12/15/15 Pct Recovery = 73% Analysis Date = 12/10/15 Pct Recovery = 73% Analysis Date = 12/10/15 Pct Recovery = 73% Analysis Date = 12/05/15 Pct Recovery = 73% Analysis Date = 12/05/15 Pct Recovery = 73% Analysis Date = 11/30/15 Pct Recovery = 73% Analysis Date = 11/30/15 Pct Recovery = 73% Analysis Date = 11/25/15 Pct Recovery = 73% Analysis Date = 11/25/15 Pct Recovery = 73% Analysis Date = 11/20/15 Pct Recovery = 73% Analysis Date = 11/20/15 Pct Recovery = 73% Analysis Date = 11/15/15 Pct Recovery = 73% Analysis Date = 11/15/15 Pct Recovery = 73% Analysis Date = 11/10/15 Pct Recovery = 73% Analysis Date = 11/10/15 Pct Recovery = 73% Analysis Date = 11/05/15 Pct Recovery = 73% Analysis Date = 11/05/15 Pct Recovery = 73% Analysis Date = 11/01/15 Pct Recovery = 73% Analysis Date = 11/01/15 Pct Recovery = 73% Analysis Date = 10/27/15 Pct Recovery = 73% Analysis Date = 10/27/15 Pct Recovery = 73% Analysis Date = 10/22/15 Pct Recovery = 73% Analysis Date = 10/22/15 Pct Recovery = 73% Analysis Date = 10/17/15 Pct Recovery = 73% Analysis Date = 10/17/15 Pct Recovery = 73% Analysis Date = 10/12/15 Pct Recovery = 73% Analysis Date = 10/12/15 Pct Recovery = 73% Analysis Date = 10/07/15 Pct Recovery = 73% Analysis Date = 10/07/15 Pct Recovery = 73% Analysis Date = 10/02/15 Pct Recovery = 73% Analysis Date = 10/02/15 Pct Recovery = 73% Analysis Date = 09/27/15 Pct Recovery = 73% Analysis Date = 09/27/15 Pct Recovery = 73% Analysis Date = 09/22/15 Pct Recovery = 73% Analysis Date = 09/22/15 Pct Recovery = 73% Analysis Date = 09/17/15 Pct Recovery = 73% Analysis Date = 09/17/15 Pct Recovery = 73% Analysis Date = 09/13/15 Pct Recovery = 73% Analysis Date = 09/13/15 Pct Recovery = 73% Analysis Date = 09/08/15 Pct Recovery = 73% Analysis Date = 09/08/15 Pct Recovery = 73% Analysis Date = 09/03/15 Pct Recovery = 73% Analysis Date = 09/03/15 Pct Recovery = 73% Analysis Date = 08/29/15 Pct Recovery = 73% Analysis Date = 08/29/15 Pct Recovery = 73% Analysis Date = 08/24/15 Pct Recovery = 73% Analysis Date = 08/24/15 Pct Recovery = 73% Analysis Date = 08/19/15 Pct Recovery = 73% Analysis Date = 08/19/15 Pct Recovery = 73% Analysis Date = 08/14/15 Pct Recovery = 73% Analysis Date = 08/14/15 Pct Recovery = 73% Analysis Date = 08/09/15 Pct Recovery = 73% Analysis Date = 08/09/15 Pct Recovery = 73% Analysis Date = 08/04/15 Pct Recovery = 73% Analysis Date = 08/04/15 Pct Recovery = 73% Analysis Date = 07/31/15 Pct Recovery = 73% Analysis Date = 07/31/15 Pct Recovery = 73% Analysis Date = 07/26/15 Pct Recovery = 73% Analysis Date = 07/26/15 Pct Recovery = 73% Analysis Date = 07/21/15 Pct Recovery = 73% Analysis Date = 07/21/15 Pct Recovery = 73% Analysis Date = 07/16/15 Pct Recovery = 73% Analysis Date = 07/16/15 Pct Recovery = 73% Analysis Date = 07/11/15 Pct Recovery = 72% Analysis Date = 07/11/15 Pct Recovery = 72% Analysis Date = 07/06/15 Pct Recovery = 72% Analysis Date = 07/06/15 Pct Recovery = 72% Analysis Date = 07/01/15 Pct Recovery = 72% Analysis Date = 07/01/15 Pct Recovery = 72% Analysis Date = 06/26/15 Pct Recovery = 72% Analysis Date = 06/26/15 Pct Recovery = 72% Analysis Date = 06/21/15 Pct Recovery = 72% Analysis Date = 06/21/15 Pct Recovery = 72% Analysis Date = 06/17/15 Pct Recovery = 72% Analysis Date = 06/17/15 Pct Recovery = 72% Analysis Date = 06/12/15 Pct Recovery = 72% Analysis Date = 06/12/15 Pct Recovery = 72% Analysis Date = 06/07/15 Pct Recovery = 72% Analysis Date = 06/07/15 Pct Recovery = 72% Analysis Date = 06/02/15 Pct Recovery = 72% Analysis Date = 06/02/15 Pct Recovery = 72% Analysis Date = 05/28/15 Pct Recovery = 72% Analysis Date = 05/28/15 Pct Recovery = 72% Analysis Date = 05/23/15 Pct Recovery = 72% Analysis Date = 05/23/15 Pct Recovery = 72% Analysis Date = 05/18/15 Pct Recovery = 72% Analysis Date = 05/18/15 Pct Recovery = 72% Analysis Date = 05/13/15 Pct Recovery = 72% Analysis Date = 05/13/15 Pct Recovery = 72% Analysis Date = 05/08/15 Pct Recovery = 72% Analysis Date = 05/08/15 Pct Recovery = 72% Analysis Date = 05/04/15 Pct Recovery = 72% Analysis Date = 05/04/15 Pct Recovery = 72% Analysis Date = 04/29/15 Pct Recovery = 72% Analysis Date = 04/29/15 Pct Recovery = 72% Analysis Date = 04/24/15 Pct Recovery = 72% Analysis Date = 04/24/15 Pct Recovery = 72% Analysis Date = 04/19/15 Pct Recovery = 72% Analysis Date = 04/19/15 Pct Recovery = 72% Analysis Date = 04/14/15 Pct Recovery = 72% Analysis Date = 04/14/15 Pct Recovery = 72% Analysis Date = 04/09/15 Pct Recovery = 72% Analysis Date = 04/09/15 Pct Recovery = 72% Analysis Date = 04/04/15 Pct Recovery = 72% Analysis Date = 04/04/15 Pct Recovery = 72% Analysis Date = 03/30/15 Pct Recovery = 72% Analysis Date = 03/30/15 Pct Recovery = 72% Analysis Date = 03/25/15 Pct Recovery = 71% Analysis Date = 03/25/15 Pct Recovery = 71% Analysis Date = 03/21/15 Pct Recovery = 71% Analysis Date = 03/21/15 Pct Recovery = 71% Analysis Date = 03/16/15 Pct Recovery = 71% Analysis Date = 03/16/15 Pct Recovery = 71% Analysis Date = 03/11/15 Pct Recovery = 71% Analysis Date = 03/11/15 Pct Recovery = 71% Analysis Date = 03/06/15 Pct Recovery = 71% Analysis Date = 03/06/15 Pct Recovery = 71% Analysis Date = 03/01/15 Pct Recovery = 70% Analysis Date = 03/01/15 Pct Recovery = 70% Analysis Date = 02/24/15 Pct Recovery = 70% Analysis Date = 02/24/15 Pct Recovery = 70% Analysis Date = 02/19/15 Pct Recovery = 70% Analysis Date = 02/19/15 Pct Recovery = 70% Analysis Date = 02/14/15 Pct Recovery = 70% Analysis Date = 02/14/15 Pct Recovery = 70% Analysis Date = 02/09/15 Pct Recovery = 70% Analysis Date = 02/09/15 Pct Recovery = 70% Analysis Date = 02/05/15 Pct Recovery = 70% Analysis Date = 02/05/15 Pct Recovery = 70% Analysis Date = 01/31/15 Pct Recovery = 69% Analysis Date = 01/31/15 Pct Recovery = 69% Analysis Date = 01/26/15 Pct Recovery = 69% Analysis Date = 01/26/15 Pct Recovery = 69% Analysis Date = 01/21/15 Pct Recovery = 69% Analysis Date = 01/21/15 Pct Recovery = 69% Analysis Date = 01/16/15 Pct Recovery = 69% Analysis Date = 01/16/15 Pct Recovery = 69% Analysis Date = 01/11/15 Pct Recovery = 69% Analysis Date = 01/11/15 Pct Recovery = 69% Analysis Date = 01/06/15 Pct Recovery = 69% Analysis Date = 01/06/15 Pct Recovery = 69% Analysis Date = 01/01/15 Pct Recovery = 68% Analysis Date = 01/01/15 Pct Recovery = 68% Analysis Date = 12/27/14 Pct Recovery = 68% Analysis Date = 12/27/14 Pct Recovery = 68% Analysis Date = 12/23/14 Pct Recovery = 68% Analysis Date = 12/23/14 Pct Recovery = 68% Analysis Date = 12/18/14 Pct Recovery = 68% Analysis Date = 12/18/14 Pct Recovery = 68% Analysis Date = 12/13/14 Pct Recovery = 68% Analysis Date = 12/13/14 Pct Recovery = 68% Analysis Date = 12/08/14 Pct Recovery = 67% Analysis Date = 12/08/14 Pct Recovery = 67% Analysis Date = 12/03/14 Pct Recovery = 67% Analysis Date = 12/03/14 Pct Recovery = 67% Analysis Date = 11/28/14 Pct Recovery = 67% Analysis Date = 11/28/14 Pct Recovery = 67% Analysis Date = 11/23/14 Pct Recovery = 67% Analysis Date = 11/23/14 Pct Recovery = 67% Analysis Date = 11/18/14 Pct Recovery = 67% Analysis Date = 11/18/14 Pct Recovery = 67% Analysis Date = 11/13/14 Pct Recovery = 67% Analysis Date = 11/13/14 Pct Recovery = 67% Analysis Date = 11/09/14 Pct Recovery = 66% Analysis Date = 11/09/14 Pct Recovery = 66% Analysis Date = 11/04/14 Pct Recovery = 66% Analysis Date = 11/04/14 Pct Recovery = 66% Analysis Date = 10/30/14 Pct Recovery = 66% Analysis Date = 10/30/14 Pct Recovery = 66% Analysis Date = 10/25/14 Pct Recovery = 66% Analysis Date = 10/25/14 Pct Recovery = 66% Analysis Date = 10/20/14 Pct Recovery = 66% Analysis Date = 10/20/14 Pct Recovery = 66% Analysis Date = 10/15/14 Pct Recovery = 66% Analysis Date = 10/15/14 Pct Recovery = 66% Analysis Date = 10/10/14 Pct Recovery = 65% Analysis Date = 10/10/14 Pct Recovery = 65% Analysis Date = 10/05/14 Pct Recovery = 65% Analysis Date = 10/05/14 Pct Recovery = 65% Analysis Date = 09/30/14 Pct Recovery = 65% Analysis Date = 09/30/14 Pct Recovery = 65% Analysis Date = 09/26/14 Pct Recovery = 65% Analysis Date = 09/26/14 Pct Recovery = 65% Analysis Date = 09/21/14 Pct Recovery = 65% Analysis Date = 09/21/14 Pct Recovery = 65% Analysis Date = 09/16/14 Pct Recovery = 64% Analysis Date = 09/16/14 Pct Recovery = 64% Analysis Date = 09/11/14 Pct Recovery = 64% Analysis Date = 09/11/14 Pct Recovery = 64% Analysis Date = 09/06/14 Pct Recovery = 64% Analysis Date = 09/06/14 Pct Recovery = 64% Analysis Date = 09/01/14 Pct Recovery = 64% Analysis Date = 09/01/14 Pct Recovery = 64% Analysis Date = 08/27/14 Pct Recovery = 64% Analysis Date = 08/27/14 Pct Recovery = 64% Analysis Date = 08/22/14 Pct Recovery = 63% Analysis Date = 08/22/14 Pct Recovery = 63% Analysis Date = 08/17/14 Pct Recovery = 63% Analysis Date = 08/17/14 Pct Recovery = 63% Analysis Date = 08/13/14 Pct Recovery = 63% Analysis Date = 08/13/14 Pct Recovery = 63% Analysis Date = 08/08/14 Pct Recovery = 63% Analysis Date = 08/08/14 Pct Recovery = 63% Analysis Date = 08/03/14 Pct Recovery = 63% Analysis Date = 08/03/14 Pct Recovery = 63% Analysis Date = 07/29/14 Pct Recovery = 62% Analysis Date = 07/29/14 Pct Recovery = 62% Analysis Date = 07/24/14 Pct Recovery = 62% Analysis Date = 07/24/14 Pct Recovery = 62% Analysis Date = 07/19/14 Pct Recovery = 62% Analysis Date = 07/19/14 Pct Recovery = 62% Analysis Date = 07/14/14 Pct Recovery = 62% Analysis Date = 07/14/14 Pct Recovery = 62% Analysis Date = 07/09/14 Pct Recovery = 62% Analysis Date = 07/09/14 Pct Recovery = 62% Analysis Date = 07/04/14 Pct Recovery = 61% Analysis Date = 07/04/14 Pct Recovery = 61% Analysis Date = 06/30/14 Pct Recovery = 61% Analysis Date = 06/30/14 Pct Recovery = 61% Analysis Date = 06/25/14 Pct Recovery = 61% Analysis Date = 06/25/14 Pct Recovery = 61% Analysis Date = 06/20/14 Pct Recovery = 61% Analysis Date = 06/20/14 Pct Recovery = 61% Analysis Date = 06/15/14 Pct Recovery = 61% Analysis Date = 06/15/14 Pct Recovery = 61% Analysis Date = 06/10/14 Pct Recovery = 60% Analysis Date = 06/10/14 Pct Recovery = 60% Analysis Date = 06/05/14 Pct Recovery = 60% Analysis Date = 06/05/14 Pct Recovery = 60% Analysis Date = 05/31/14 Pct Recovery = 60% Analysis Date = 05/31/14 Pct Recovery = 60% Analysis Date = 05/26/14 Pct Recovery = 60% Analysis Date = 05/26/14 Pct Recovery = 60% Analysis Date = 05/21/14 Pct Recovery = 60% Analysis Date = 05/21/14 Pct Recovery = 60% Analysis Date = 05/17/14 Pct Recovery = 59% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
DIPHENHYDRAMINE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 6 92% 31% 82% 37%
>= Reporting Level 56 70% 10% 69% 10%
Total 62 72% 14% 69% 10%

Sample Statistics
DIPHENHYDRAMINE

Characteristic N % % Basis
Plotted 62 82% Spiked
Estimated Values 24 32% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 4 5% Spiked
Spiked 76 .  
False Negatives 10 13% 10 out of 76
Not Spiked 39 .  
False Positives 0 0% 0 out of 39

BQS OBSP Determination:
DULOXETINE
METHOD: 2440 , TESTIDCODE: 67448LCM56
Open Data Set

Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 39% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 52% Analysis Date = 01/17/16 SpikeMix = ERA 0406-15-09: 80 µl & ERA 0406-15-07A: 80 µl Pct Recovery = 64% Analysis Date = 11/24/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 70% Analysis Date = 10/01/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 68% Analysis Date = 11/05/15 SpikeMix = ERA 0406-15-08: 80 µl & Abs 052215: 80 µl Pct Recovery = 64% Analysis Date = 11/04/15 SpikeMix = Abs 052215: 80 µl & Abs 050115: 80 µl Pct Recovery = 46% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 53% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 53% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 59% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 66% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-04: 15 µl & Abs 041814: 15 µl Pct Recovery = 50% Analysis Date = 12/06/14 SpikeMix = ERA 0318-14-02: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 55% Analysis Date = 10/25/14 SpikeMix = Abs 041614: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 56% Analysis Date = 10/11/14 SpikeMix = ERA 0318-14-02: 60 µl & ERA 0319-14-04: 60 µl Pct Recovery = 60% Analysis Date = 08/28/14 SpikeMix = ERA 0319-14-04: 60 µl & ERA 0319-14-05: 60 µl Pct Recovery = 49% Analysis Date = 05/07/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 44% Analysis Date = 03/11/15 SpikeMix = ERA 0318-14-02: 15 µl & Abs 041714: 15 µl Pct Recovery = 55% Analysis Date = 01/16/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 58% Analysis Date = 12/06/14 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 53% Analysis Date = 08/21/14 SpikeMix = ERA 0318-14-02: 60 µl & Abs 041714: 60 µl Pct Recovery = 29% Analysis Date = 07/12/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 52% Analysis Date = 06/11/14 SpikeMix = Abs 041614: 60 µl & Abs 041714: 60 µl Pct Recovery = 39% Analysis Date = 05/21/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 53% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-08: 40 µl & ERA 0406-15-09: 40 µl Pct Recovery = 57% Analysis Date = 07/31/15 SpikeMix = ERA 0406-15-09: 40 µl & Abs 050115: 40 µl Pct Recovery = 78% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-08: 40 µl & Abs 052215: 40 µl Pct Recovery = 68% Analysis Date = 02/23/16 SpikeMix = Abs 052215: 40 µl & Abs 050115: 40 µl Pct Recovery = 72% Analysis Date = 09/10/15 SpikeMix = Abs 052215: 40 µl & ERA 0406-15-07A: 40 µl Pct Recovery = 63% Analysis Date = 07/31/15 SpikeMix = Abs 051315: 40 µl & Abs 052215: 40 µl Pct Recovery = 54% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 51% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 51% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 42% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 52% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 22% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 46% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 37% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 48% Analysis Date = 04/30/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 65% Analysis Date = 02/10/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 30% Analysis Date = 12/07/14 SpikeMix = ERA 0318-14-02: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 71% Analysis Date = 10/11/14 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 44% Analysis Date = 11/04/14 SpikeMix = Abs 041714: 8 µl & ERA 0319-14-05: 8 µl Pct Recovery = 32% Analysis Date = 09/12/14 SpikeMix = Abs 041614: 30 µl & ERA 0319-14-04: 30 µl Pct Recovery = 44% Analysis Date = 08/16/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 34% Analysis Date = 07/13/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 25% Analysis Date = 07/20/14 SpikeMix = ERA 0318-14-02: 30 µl & Abs 041714: 30 µl Pct Recovery = 24% Analysis Date = 06/28/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 48% Analysis Date = 05/17/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 56% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 69% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-08: 20 µl & ERA 0406-15-09: 20 µl Pct Recovery = 60% Analysis Date = 11/24/15 SpikeMix = ERA 0406-15-09: 20 µl & Abs 050115: 20 µl Pct Recovery = 62% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 54% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 54% Analysis Date = 02/23/16 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 67% Analysis Date = 11/24/15 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 57% Analysis Date = 09/09/15 SpikeMix = ERA 0406-15-08: 20 µl & Abs 052215: 20 µl Pct Recovery = 58% Analysis Date = 07/09/15 SpikeMix = Abs 050115: 20 µl & Abs 052215: 20 µl Pct Recovery = 51% Analysis Date = 06/26/15 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 114% Analysis Date = 01/18/17 Pct Recovery = 42% Analysis Date = 01/14/17 Pct Recovery = 43% Analysis Date = 01/14/17 Pct Recovery = 43% Analysis Date = 01/09/17 Pct Recovery = 43% Analysis Date = 01/09/17 Pct Recovery = 43% Analysis Date = 01/04/17 Pct Recovery = 43% Analysis Date = 01/04/17 Pct Recovery = 43% Analysis Date = 12/30/16 Pct Recovery = 44% Analysis Date = 12/30/16 Pct Recovery = 44% Analysis Date = 12/25/16 Pct Recovery = 44% Analysis Date = 12/25/16 Pct Recovery = 44% Analysis Date = 12/20/16 Pct Recovery = 44% Analysis Date = 12/20/16 Pct Recovery = 44% Analysis Date = 12/15/16 Pct Recovery = 44% Analysis Date = 12/15/16 Pct Recovery = 44% Analysis Date = 12/10/16 Pct Recovery = 45% Analysis Date = 12/10/16 Pct Recovery = 45% Analysis Date = 12/05/16 Pct Recovery = 45% Analysis Date = 12/05/16 Pct Recovery = 45% Analysis Date = 12/01/16 Pct Recovery = 45% Analysis Date = 12/01/16 Pct Recovery = 45% Analysis Date = 11/26/16 Pct Recovery = 45% Analysis Date = 11/26/16 Pct Recovery = 45% Analysis Date = 11/21/16 Pct Recovery = 46% Analysis Date = 11/21/16 Pct Recovery = 46% Analysis Date = 11/16/16 Pct Recovery = 46% Analysis Date = 11/16/16 Pct Recovery = 46% Analysis Date = 11/11/16 Pct Recovery = 46% Analysis Date = 11/11/16 Pct Recovery = 46% Analysis Date = 11/06/16 Pct Recovery = 46% Analysis Date = 11/06/16 Pct Recovery = 46% Analysis Date = 11/01/16 Pct Recovery = 47% Analysis Date = 11/01/16 Pct Recovery = 47% Analysis Date = 10/27/16 Pct Recovery = 47% Analysis Date = 10/27/16 Pct Recovery = 47% Analysis Date = 10/22/16 Pct Recovery = 47% Analysis Date = 10/22/16 Pct Recovery = 47% Analysis Date = 10/18/16 Pct Recovery = 47% Analysis Date = 10/18/16 Pct Recovery = 47% Analysis Date = 10/13/16 Pct Recovery = 48% Analysis Date = 10/13/16 Pct Recovery = 48% Analysis Date = 10/08/16 Pct Recovery = 48% Analysis Date = 10/08/16 Pct Recovery = 48% Analysis Date = 10/03/16 Pct Recovery = 48% Analysis Date = 10/03/16 Pct Recovery = 48% Analysis Date = 09/28/16 Pct Recovery = 48% Analysis Date = 09/28/16 Pct Recovery = 48% Analysis Date = 09/23/16 Pct Recovery = 49% Analysis Date = 09/23/16 Pct Recovery = 49% Analysis Date = 09/18/16 Pct Recovery = 49% Analysis Date = 09/18/16 Pct Recovery = 49% Analysis Date = 09/13/16 Pct Recovery = 49% Analysis Date = 09/13/16 Pct Recovery = 49% Analysis Date = 09/08/16 Pct Recovery = 49% Analysis Date = 09/08/16 Pct Recovery = 49% Analysis Date = 09/04/16 Pct Recovery = 50% Analysis Date = 09/04/16 Pct Recovery = 50% Analysis Date = 08/30/16 Pct Recovery = 50% Analysis Date = 08/30/16 Pct Recovery = 50% Analysis Date = 08/25/16 Pct Recovery = 50% Analysis Date = 08/25/16 Pct Recovery = 50% Analysis Date = 08/20/16 Pct Recovery = 50% Analysis Date = 08/20/16 Pct Recovery = 50% Analysis Date = 08/15/16 Pct Recovery = 51% Analysis Date = 08/15/16 Pct Recovery = 51% Analysis Date = 08/10/16 Pct Recovery = 51% Analysis Date = 08/10/16 Pct Recovery = 51% Analysis Date = 08/05/16 Pct Recovery = 51% Analysis Date = 08/05/16 Pct Recovery = 51% Analysis Date = 07/31/16 Pct Recovery = 51% Analysis Date = 07/31/16 Pct Recovery = 51% Analysis Date = 07/26/16 Pct Recovery = 52% Analysis Date = 07/26/16 Pct Recovery = 52% Analysis Date = 07/22/16 Pct Recovery = 52% Analysis Date = 07/22/16 Pct Recovery = 52% Analysis Date = 07/17/16 Pct Recovery = 52% Analysis Date = 07/17/16 Pct Recovery = 52% Analysis Date = 07/12/16 Pct Recovery = 52% Analysis Date = 07/12/16 Pct Recovery = 52% Analysis Date = 07/07/16 Pct Recovery = 53% Analysis Date = 07/07/16 Pct Recovery = 53% Analysis Date = 07/02/16 Pct Recovery = 53% Analysis Date = 07/02/16 Pct Recovery = 53% Analysis Date = 06/27/16 Pct Recovery = 53% Analysis Date = 06/27/16 Pct Recovery = 53% Analysis Date = 06/22/16 Pct Recovery = 53% Analysis Date = 06/22/16 Pct Recovery = 53% Analysis Date = 06/17/16 Pct Recovery = 54% Analysis Date = 06/17/16 Pct Recovery = 54% Analysis Date = 06/12/16 Pct Recovery = 54% Analysis Date = 06/12/16 Pct Recovery = 54% Analysis Date = 06/08/16 Pct Recovery = 54% Analysis Date = 06/08/16 Pct Recovery = 54% Analysis Date = 06/03/16 Pct Recovery = 54% Analysis Date = 06/03/16 Pct Recovery = 54% Analysis Date = 05/29/16 Pct Recovery = 54% Analysis Date = 05/29/16 Pct Recovery = 54% Analysis Date = 05/24/16 Pct Recovery = 55% Analysis Date = 05/24/16 Pct Recovery = 55% Analysis Date = 05/19/16 Pct Recovery = 55% Analysis Date = 05/19/16 Pct Recovery = 55% Analysis Date = 05/14/16 Pct Recovery = 55% Analysis Date = 05/14/16 Pct Recovery = 55% Analysis Date = 05/09/16 Pct Recovery = 55% Analysis Date = 05/09/16 Pct Recovery = 55% Analysis Date = 05/04/16 Pct Recovery = 56% Analysis Date = 05/04/16 Pct Recovery = 56% Analysis Date = 04/29/16 Pct Recovery = 56% Analysis Date = 04/29/16 Pct Recovery = 56% Analysis Date = 04/25/16 Pct Recovery = 56% Analysis Date = 04/25/16 Pct Recovery = 56% Analysis Date = 04/20/16 Pct Recovery = 56% Analysis Date = 04/20/16 Pct Recovery = 56% Analysis Date = 04/15/16 Pct Recovery = 57% Analysis Date = 04/15/16 Pct Recovery = 57% Analysis Date = 04/10/16 Pct Recovery = 57% Analysis Date = 04/10/16 Pct Recovery = 57% Analysis Date = 04/05/16 Pct Recovery = 57% Analysis Date = 04/05/16 Pct Recovery = 57% Analysis Date = 03/31/16 Pct Recovery = 57% Analysis Date = 03/31/16 Pct Recovery = 57% Analysis Date = 03/26/16 Pct Recovery = 58% Analysis Date = 03/26/16 Pct Recovery = 58% Analysis Date = 03/21/16 Pct Recovery = 58% Analysis Date = 03/21/16 Pct Recovery = 58% Analysis Date = 03/16/16 Pct Recovery = 58% Analysis Date = 03/16/16 Pct Recovery = 58% Analysis Date = 03/12/16 Pct Recovery = 58% Analysis Date = 03/12/16 Pct Recovery = 58% Analysis Date = 03/07/16 Pct Recovery = 59% Analysis Date = 03/07/16 Pct Recovery = 59% Analysis Date = 03/02/16 Pct Recovery = 59% Analysis Date = 03/02/16 Pct Recovery = 59% Analysis Date = 02/26/16 Pct Recovery = 59% Analysis Date = 02/26/16 Pct Recovery = 59% Analysis Date = 02/21/16 Pct Recovery = 59% Analysis Date = 02/21/16 Pct Recovery = 59% Analysis Date = 02/16/16 Pct Recovery = 60% Analysis Date = 02/16/16 Pct Recovery = 60% Analysis Date = 02/11/16 Pct Recovery = 60% Analysis Date = 02/11/16 Pct Recovery = 60% Analysis Date = 02/06/16 Pct Recovery = 60% Analysis Date = 02/06/16 Pct Recovery = 60% Analysis Date = 02/01/16 Pct Recovery = 60% Analysis Date = 02/01/16 Pct Recovery = 60% Analysis Date = 01/28/16 Pct Recovery = 61% Analysis Date = 01/28/16 Pct Recovery = 61% Analysis Date = 01/23/16 Pct Recovery = 61% Analysis Date = 01/23/16 Pct Recovery = 61% Analysis Date = 01/18/16 Pct Recovery = 61% Analysis Date = 01/18/16 Pct Recovery = 61% Analysis Date = 01/13/16 Pct Recovery = 61% Analysis Date = 01/13/16 Pct Recovery = 61% Analysis Date = 01/08/16 Pct Recovery = 62% Analysis Date = 01/08/16 Pct Recovery = 62% Analysis Date = 01/03/16 Pct Recovery = 62% Analysis Date = 01/03/16 Pct Recovery = 62% Analysis Date = 12/29/15 Pct Recovery = 62% Analysis Date = 12/29/15 Pct Recovery = 62% Analysis Date = 12/24/15 Pct Recovery = 62% Analysis Date = 12/24/15 Pct Recovery = 62% Analysis Date = 12/19/15 Pct Recovery = 63% Analysis Date = 12/19/15 Pct Recovery = 63% Analysis Date = 12/15/15 Pct Recovery = 63% Analysis Date = 12/15/15 Pct Recovery = 63% Analysis Date = 12/10/15 Pct Recovery = 63% Analysis Date = 12/10/15 Pct Recovery = 63% Analysis Date = 12/05/15 Pct Recovery = 63% Analysis Date = 12/05/15 Pct Recovery = 63% Analysis Date = 11/30/15 Pct Recovery = 63% Analysis Date = 11/30/15 Pct Recovery = 63% Analysis Date = 11/25/15 Pct Recovery = 63% Analysis Date = 11/25/15 Pct Recovery = 63% Analysis Date = 11/20/15 Pct Recovery = 63% Analysis Date = 11/20/15 Pct Recovery = 63% Analysis Date = 11/15/15 Pct Recovery = 63% Analysis Date = 11/15/15 Pct Recovery = 63% Analysis Date = 11/10/15 Pct Recovery = 63% Analysis Date = 11/10/15 Pct Recovery = 63% Analysis Date = 11/05/15 Pct Recovery = 63% Analysis Date = 11/05/15 Pct Recovery = 63% Analysis Date = 11/01/15 Pct Recovery = 63% Analysis Date = 11/01/15 Pct Recovery = 63% Analysis Date = 10/27/15 Pct Recovery = 63% Analysis Date = 10/27/15 Pct Recovery = 63% Analysis Date = 10/22/15 Pct Recovery = 63% Analysis Date = 10/22/15 Pct Recovery = 63% Analysis Date = 10/17/15 Pct Recovery = 63% Analysis Date = 10/17/15 Pct Recovery = 63% Analysis Date = 10/12/15 Pct Recovery = 63% Analysis Date = 10/12/15 Pct Recovery = 63% Analysis Date = 10/07/15 Pct Recovery = 63% Analysis Date = 10/07/15 Pct Recovery = 63% Analysis Date = 10/02/15 Pct Recovery = 63% Analysis Date = 10/02/15 Pct Recovery = 63% Analysis Date = 09/27/15 Pct Recovery = 63% Analysis Date = 09/27/15 Pct Recovery = 63% Analysis Date = 09/22/15 Pct Recovery = 62% Analysis Date = 09/22/15 Pct Recovery = 62% Analysis Date = 09/17/15 Pct Recovery = 62% Analysis Date = 09/17/15 Pct Recovery = 62% Analysis Date = 09/13/15 Pct Recovery = 62% Analysis Date = 09/13/15 Pct Recovery = 62% Analysis Date = 09/08/15 Pct Recovery = 62% Analysis Date = 09/08/15 Pct Recovery = 62% Analysis Date = 09/03/15 Pct Recovery = 62% Analysis Date = 09/03/15 Pct Recovery = 62% Analysis Date = 08/29/15 Pct Recovery = 62% Analysis Date = 08/29/15 Pct Recovery = 62% Analysis Date = 08/24/15 Pct Recovery = 62% Analysis Date = 08/24/15 Pct Recovery = 62% Analysis Date = 08/19/15 Pct Recovery = 62% Analysis Date = 08/19/15 Pct Recovery = 62% Analysis Date = 08/14/15 Pct Recovery = 61% Analysis Date = 08/14/15 Pct Recovery = 61% Analysis Date = 08/09/15 Pct Recovery = 61% Analysis Date = 08/09/15 Pct Recovery = 61% Analysis Date = 08/04/15 Pct Recovery = 61% Analysis Date = 08/04/15 Pct Recovery = 61% Analysis Date = 07/31/15 Pct Recovery = 61% Analysis Date = 07/31/15 Pct Recovery = 61% Analysis Date = 07/26/15 Pct Recovery = 61% Analysis Date = 07/26/15 Pct Recovery = 61% Analysis Date = 07/21/15 Pct Recovery = 61% Analysis Date = 07/21/15 Pct Recovery = 61% Analysis Date = 07/16/15 Pct Recovery = 61% Analysis Date = 07/16/15 Pct Recovery = 61% Analysis Date = 07/11/15 Pct Recovery = 60% Analysis Date = 07/11/15 Pct Recovery = 60% Analysis Date = 07/06/15 Pct Recovery = 60% Analysis Date = 07/06/15 Pct Recovery = 60% Analysis Date = 07/01/15 Pct Recovery = 60% Analysis Date = 07/01/15 Pct Recovery = 60% Analysis Date = 06/26/15 Pct Recovery = 60% Analysis Date = 06/26/15 Pct Recovery = 60% Analysis Date = 06/21/15 Pct Recovery = 60% Analysis Date = 06/21/15 Pct Recovery = 60% Analysis Date = 06/17/15 Pct Recovery = 60% Analysis Date = 06/17/15 Pct Recovery = 60% Analysis Date = 06/12/15 Pct Recovery = 60% Analysis Date = 06/12/15 Pct Recovery = 60% Analysis Date = 06/07/15 Pct Recovery = 59% Analysis Date = 06/07/15 Pct Recovery = 59% Analysis Date = 06/02/15 Pct Recovery = 59% Analysis Date = 06/02/15 Pct Recovery = 59% Analysis Date = 05/28/15 Pct Recovery = 59% Analysis Date = 05/28/15 Pct Recovery = 59% Analysis Date = 05/23/15 Pct Recovery = 59% Analysis Date = 05/23/15 Pct Recovery = 59% Analysis Date = 05/18/15 Pct Recovery = 59% Analysis Date = 05/18/15 Pct Recovery = 59% Analysis Date = 05/13/15 Pct Recovery = 59% Analysis Date = 05/13/15 Pct Recovery = 59% Analysis Date = 05/08/15 Pct Recovery = 59% Analysis Date = 05/08/15 Pct Recovery = 59% Analysis Date = 05/04/15 Pct Recovery = 58% Analysis Date = 05/04/15 Pct Recovery = 58% Analysis Date = 04/29/15 Pct Recovery = 58% Analysis Date = 04/29/15 Pct Recovery = 58% Analysis Date = 04/24/15 Pct Recovery = 58% Analysis Date = 04/24/15 Pct Recovery = 58% Analysis Date = 04/19/15 Pct Recovery = 58% Analysis Date = 04/19/15 Pct Recovery = 58% Analysis Date = 04/14/15 Pct Recovery = 58% Analysis Date = 04/14/15 Pct Recovery = 58% Analysis Date = 04/09/15 Pct Recovery = 57% Analysis Date = 04/09/15 Pct Recovery = 57% Analysis Date = 04/04/15 Pct Recovery = 57% Analysis Date = 04/04/15 Pct Recovery = 57% Analysis Date = 03/30/15 Pct Recovery = 57% Analysis Date = 03/30/15 Pct Recovery = 57% Analysis Date = 03/25/15 Pct Recovery = 57% Analysis Date = 03/25/15 Pct Recovery = 57% Analysis Date = 03/21/15 Pct Recovery = 56% Analysis Date = 03/21/15 Pct Recovery = 56% Analysis Date = 03/16/15 Pct Recovery = 56% Analysis Date = 03/16/15 Pct Recovery = 56% Analysis Date = 03/11/15 Pct Recovery = 56% Analysis Date = 03/11/15 Pct Recovery = 56% Analysis Date = 03/06/15 Pct Recovery = 56% Analysis Date = 03/06/15 Pct Recovery = 56% Analysis Date = 03/01/15 Pct Recovery = 55% Analysis Date = 03/01/15 Pct Recovery = 55% Analysis Date = 02/24/15 Pct Recovery = 55% Analysis Date = 02/24/15 Pct Recovery = 55% Analysis Date = 02/19/15 Pct Recovery = 55% Analysis Date = 02/19/15 Pct Recovery = 55% Analysis Date = 02/14/15 Pct Recovery = 55% Analysis Date = 02/14/15 Pct Recovery = 55% Analysis Date = 02/09/15 Pct Recovery = 54% Analysis Date = 02/09/15 Pct Recovery = 54% Analysis Date = 02/05/15 Pct Recovery = 54% Analysis Date = 02/05/15 Pct Recovery = 54% Analysis Date = 01/31/15 Pct Recovery = 54% Analysis Date = 01/31/15 Pct Recovery = 54% Analysis Date = 01/26/15 Pct Recovery = 53% Analysis Date = 01/26/15 Pct Recovery = 53% Analysis Date = 01/21/15 Pct Recovery = 53% Analysis Date = 01/21/15 Pct Recovery = 53% Analysis Date = 01/16/15 Pct Recovery = 53% Analysis Date = 01/16/15 Pct Recovery = 53% Analysis Date = 01/11/15 Pct Recovery = 53% Analysis Date = 01/11/15 Pct Recovery = 53% Analysis Date = 01/06/15 Pct Recovery = 52% Analysis Date = 01/06/15 Pct Recovery = 52% Analysis Date = 01/01/15 Pct Recovery = 52% Analysis Date = 01/01/15 Pct Recovery = 52% Analysis Date = 12/27/14 Pct Recovery = 52% Analysis Date = 12/27/14 Pct Recovery = 52% Analysis Date = 12/23/14 Pct Recovery = 52% Analysis Date = 12/23/14 Pct Recovery = 52% Analysis Date = 12/18/14 Pct Recovery = 51% Analysis Date = 12/18/14 Pct Recovery = 51% Analysis Date = 12/13/14 Pct Recovery = 51% Analysis Date = 12/13/14 Pct Recovery = 51% Analysis Date = 12/08/14 Pct Recovery = 51% Analysis Date = 12/08/14 Pct Recovery = 51% Analysis Date = 12/03/14 Pct Recovery = 50% Analysis Date = 12/03/14 Pct Recovery = 50% Analysis Date = 11/28/14 Pct Recovery = 50% Analysis Date = 11/28/14 Pct Recovery = 50% Analysis Date = 11/23/14 Pct Recovery = 50% Analysis Date = 11/23/14 Pct Recovery = 50% Analysis Date = 11/18/14 Pct Recovery = 49% Analysis Date = 11/18/14 Pct Recovery = 49% Analysis Date = 11/13/14 Pct Recovery = 49% Analysis Date = 11/13/14 Pct Recovery = 49% Analysis Date = 11/09/14 Pct Recovery = 49% Analysis Date = 11/09/14 Pct Recovery = 49% Analysis Date = 11/04/14 Pct Recovery = 49% Analysis Date = 11/04/14 Pct Recovery = 49% Analysis Date = 10/30/14 Pct Recovery = 48% Analysis Date = 10/30/14 Pct Recovery = 48% Analysis Date = 10/25/14 Pct Recovery = 48% Analysis Date = 10/25/14 Pct Recovery = 48% Analysis Date = 10/20/14 Pct Recovery = 48% Analysis Date = 10/20/14 Pct Recovery = 48% Analysis Date = 10/15/14 Pct Recovery = 47% Analysis Date = 10/15/14 Pct Recovery = 47% Analysis Date = 10/10/14 Pct Recovery = 47% Analysis Date = 10/10/14 Pct Recovery = 47% Analysis Date = 10/05/14 Pct Recovery = 47% Analysis Date = 10/05/14 Pct Recovery = 47% Analysis Date = 09/30/14 Pct Recovery = 47% Analysis Date = 09/30/14 Pct Recovery = 47% Analysis Date = 09/26/14 Pct Recovery = 46% Analysis Date = 09/26/14 Pct Recovery = 46% Analysis Date = 09/21/14 Pct Recovery = 46% Analysis Date = 09/21/14 Pct Recovery = 46% Analysis Date = 09/16/14 Pct Recovery = 46% Analysis Date = 09/16/14 Pct Recovery = 46% Analysis Date = 09/11/14 Pct Recovery = 46% Analysis Date = 09/11/14 Pct Recovery = 46% Analysis Date = 09/06/14 Pct Recovery = 45% Analysis Date = 09/06/14 Pct Recovery = 45% Analysis Date = 09/01/14 Pct Recovery = 45% Analysis Date = 09/01/14 Pct Recovery = 45% Analysis Date = 08/27/14 Pct Recovery = 45% Analysis Date = 08/27/14 Pct Recovery = 45% Analysis Date = 08/22/14 Pct Recovery = 45% Analysis Date = 08/22/14 Pct Recovery = 45% Analysis Date = 08/17/14 Pct Recovery = 44% Analysis Date = 08/17/14 Pct Recovery = 44% Analysis Date = 08/13/14 Pct Recovery = 44% Analysis Date = 08/13/14 Pct Recovery = 44% Analysis Date = 08/08/14 Pct Recovery = 44% Analysis Date = 08/08/14 Pct Recovery = 44% Analysis Date = 08/03/14 Pct Recovery = 44% Analysis Date = 08/03/14 Pct Recovery = 44% Analysis Date = 07/29/14 Pct Recovery = 43% Analysis Date = 07/29/14 Pct Recovery = 43% Analysis Date = 07/24/14 Pct Recovery = 43% Analysis Date = 07/24/14 Pct Recovery = 43% Analysis Date = 07/19/14 Pct Recovery = 43% Analysis Date = 07/19/14 Pct Recovery = 43% Analysis Date = 07/14/14 Pct Recovery = 43% Analysis Date = 07/14/14 Pct Recovery = 43% Analysis Date = 07/09/14 Pct Recovery = 42% Analysis Date = 07/09/14 Pct Recovery = 42% Analysis Date = 07/04/14 Pct Recovery = 42% Analysis Date = 07/04/14 Pct Recovery = 42% Analysis Date = 06/30/14 Pct Recovery = 42% Analysis Date = 06/30/14 Pct Recovery = 42% Analysis Date = 06/25/14 Pct Recovery = 42% Analysis Date = 06/25/14 Pct Recovery = 42% Analysis Date = 06/20/14 Pct Recovery = 41% Analysis Date = 06/20/14 Pct Recovery = 41% Analysis Date = 06/15/14 Pct Recovery = 41% Analysis Date = 06/15/14 Pct Recovery = 41% Analysis Date = 06/10/14 Pct Recovery = 41% Analysis Date = 06/10/14 Pct Recovery = 41% Analysis Date = 06/05/14 Pct Recovery = 41% Analysis Date = 06/05/14 Pct Recovery = 41% Analysis Date = 05/31/14 Pct Recovery = 40% Analysis Date = 05/31/14 Pct Recovery = 40% Analysis Date = 05/26/14 Pct Recovery = 40% Analysis Date = 05/26/14 Pct Recovery = 40% Analysis Date = 05/21/14 Pct Recovery = 40% Analysis Date = 05/21/14 Pct Recovery = 40% Analysis Date = 05/17/14 Pct Recovery = 40% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
DULOXETINE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 59 53% 15% 53% 12%
Total 59 53% 15% 53% 12%

Sample Statistics
DULOXETINE

Characteristic N % % Basis
Plotted 59 89% Spiked
Estimated Values 55 83% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 2 3% Spiked
Spiked 66 .  
False Negatives 5 8% 5 out of 66
Not Spiked 49 .  
False Positives 0 0% 0 out of 49

BQS OBSP Determination:
ERYTHROMYCIN
METHOD: 2440 , TESTIDCODE: 67449LCM56
Open Data Set

Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 14% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 12% Analysis Date = 11/18/16 SpikeMix = ERA 04281604: 80 µl & ERA 04281603: 80 µl Pct Recovery = 12% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & ERA 04281604: 80 µl Pct Recovery = 12% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-04: 15 µl & Abs 041814: 15 µl Pct Recovery = 41% Analysis Date = 02/06/15 SpikeMix = Abs 041814: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 47% Analysis Date = 07/12/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 50% Analysis Date = 06/22/14 SpikeMix = Abs 041814: 60 µl & Abs 041614: 60 µl Pct Recovery = 65% Analysis Date = 05/21/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 57% Analysis Date = 05/07/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 50% Analysis Date = 04/29/15 SpikeMix = ERA 0319-14-05: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 65% Analysis Date = 01/16/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 47% Analysis Date = 12/07/14 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 54% Analysis Date = 12/06/14 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 43% Analysis Date = 08/28/14 SpikeMix = ERA 0319-14-04: 60 µl & ERA 0319-14-05: 60 µl Pct Recovery = 35% Analysis Date = 07/26/14 SpikeMix = ERA 0319-14-05: 60 µl & ERA 0318-14-02: 60 µl Pct Recovery = 65% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 21% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 19% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 16% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 23% Analysis Date = 11/04/14 SpikeMix = Abs 041814: 8 µl & ERA 0318-14-02: 8 µl Pct Recovery = 23% Analysis Date = 10/11/14 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 37% Analysis Date = 11/04/14 SpikeMix = Abs 041714: 8 µl & ERA 0319-14-05: 8 µl Pct Recovery = 18% Analysis Date = 10/24/14 SpikeMix = ERA 0319-14-05: 8 µl & Abs 041614: 8 µl Pct Recovery = 23% Analysis Date = 10/10/14 SpikeMix = Abs 041714: 30 µl & Abs 041814: 30 µl Pct Recovery = 57% Analysis Date = 10/10/14 SpikeMix = Abs 041814: 30 µl & ERA 0318-14-02: 30 µl Pct Recovery = 56% Analysis Date = 07/13/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 36% Analysis Date = 05/30/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 49% Analysis Date = 08/30/14 SpikeMix = ERA 0318-14-02: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 52% Analysis Date = 08/16/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 31% Analysis Date = 07/13/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 17% Analysis Date = 11/18/16 Pct Recovery = 14% Analysis Date = 11/13/16 Pct Recovery = 15% Analysis Date = 11/13/16 Pct Recovery = 15% Analysis Date = 11/08/16 Pct Recovery = 15% Analysis Date = 11/08/16 Pct Recovery = 15% Analysis Date = 11/04/16 Pct Recovery = 15% Analysis Date = 11/04/16 Pct Recovery = 15% Analysis Date = 10/30/16 Pct Recovery = 16% Analysis Date = 10/30/16 Pct Recovery = 16% Analysis Date = 10/26/16 Pct Recovery = 16% Analysis Date = 10/26/16 Pct Recovery = 16% Analysis Date = 10/21/16 Pct Recovery = 16% Analysis Date = 10/21/16 Pct Recovery = 16% Analysis Date = 10/17/16 Pct Recovery = 17% Analysis Date = 10/17/16 Pct Recovery = 17% Analysis Date = 10/12/16 Pct Recovery = 17% Analysis Date = 10/12/16 Pct Recovery = 17% Analysis Date = 10/07/16 Pct Recovery = 17% Analysis Date = 10/07/16 Pct Recovery = 17% Analysis Date = 10/03/16 Pct Recovery = 17% Analysis Date = 10/03/16 Pct Recovery = 17% Analysis Date = 09/28/16 Pct Recovery = 18% Analysis Date = 09/28/16 Pct Recovery = 18% Analysis Date = 09/24/16 Pct Recovery = 18% Analysis Date = 09/24/16 Pct Recovery = 18% Analysis Date = 09/19/16 Pct Recovery = 18% Analysis Date = 09/19/16 Pct Recovery = 18% Analysis Date = 09/15/16 Pct Recovery = 19% Analysis Date = 09/15/16 Pct Recovery = 19% Analysis Date = 09/10/16 Pct Recovery = 19% Analysis Date = 09/10/16 Pct Recovery = 19% Analysis Date = 09/06/16 Pct Recovery = 19% Analysis Date = 09/06/16 Pct Recovery = 19% Analysis Date = 09/01/16 Pct Recovery = 20% Analysis Date = 09/01/16 Pct Recovery = 20% Analysis Date = 08/27/16 Pct Recovery = 20% Analysis Date = 08/27/16 Pct Recovery = 20% Analysis Date = 08/23/16 Pct Recovery = 20% Analysis Date = 08/23/16 Pct Recovery = 20% Analysis Date = 08/18/16 Pct Recovery = 21% Analysis Date = 08/18/16 Pct Recovery = 21% Analysis Date = 08/14/16 Pct Recovery = 21% Analysis Date = 08/14/16 Pct Recovery = 21% Analysis Date = 08/09/16 Pct Recovery = 21% Analysis Date = 08/09/16 Pct Recovery = 21% Analysis Date = 08/05/16 Pct Recovery = 21% Analysis Date = 08/05/16 Pct Recovery = 21% Analysis Date = 07/31/16 Pct Recovery = 22% Analysis Date = 07/31/16 Pct Recovery = 22% Analysis Date = 07/27/16 Pct Recovery = 22% Analysis Date = 07/27/16 Pct Recovery = 22% Analysis Date = 07/22/16 Pct Recovery = 22% Analysis Date = 07/22/16 Pct Recovery = 22% Analysis Date = 07/17/16 Pct Recovery = 23% Analysis Date = 07/17/16 Pct Recovery = 23% Analysis Date = 07/13/16 Pct Recovery = 23% Analysis Date = 07/13/16 Pct Recovery = 23% Analysis Date = 07/08/16 Pct Recovery = 23% Analysis Date = 07/08/16 Pct Recovery = 23% Analysis Date = 07/04/16 Pct Recovery = 24% Analysis Date = 07/04/16 Pct Recovery = 24% Analysis Date = 06/29/16 Pct Recovery = 24% Analysis Date = 06/29/16 Pct Recovery = 24% Analysis Date = 06/25/16 Pct Recovery = 24% Analysis Date = 06/25/16 Pct Recovery = 24% Analysis Date = 06/20/16 Pct Recovery = 25% Analysis Date = 06/20/16 Pct Recovery = 25% Analysis Date = 06/15/16 Pct Recovery = 25% Analysis Date = 06/15/16 Pct Recovery = 25% Analysis Date = 06/11/16 Pct Recovery = 25% Analysis Date = 06/11/16 Pct Recovery = 25% Analysis Date = 06/06/16 Pct Recovery = 26% Analysis Date = 06/06/16 Pct Recovery = 26% Analysis Date = 06/02/16 Pct Recovery = 26% Analysis Date = 06/02/16 Pct Recovery = 26% Analysis Date = 05/28/16 Pct Recovery = 26% Analysis Date = 05/28/16 Pct Recovery = 26% Analysis Date = 05/24/16 Pct Recovery = 27% Analysis Date = 05/24/16 Pct Recovery = 27% Analysis Date = 05/19/16 Pct Recovery = 27% Analysis Date = 05/19/16 Pct Recovery = 27% Analysis Date = 05/15/16 Pct Recovery = 27% Analysis Date = 05/15/16 Pct Recovery = 27% Analysis Date = 05/10/16 Pct Recovery = 28% Analysis Date = 05/10/16 Pct Recovery = 28% Analysis Date = 05/05/16 Pct Recovery = 28% Analysis Date = 05/05/16 Pct Recovery = 28% Analysis Date = 05/01/16 Pct Recovery = 28% Analysis Date = 05/01/16 Pct Recovery = 28% Analysis Date = 04/26/16 Pct Recovery = 28% Analysis Date = 04/26/16 Pct Recovery = 28% Analysis Date = 04/22/16 Pct Recovery = 29% Analysis Date = 04/22/16 Pct Recovery = 29% Analysis Date = 04/17/16 Pct Recovery = 29% Analysis Date = 04/17/16 Pct Recovery = 29% Analysis Date = 04/13/16 Pct Recovery = 29% Analysis Date = 04/13/16 Pct Recovery = 29% Analysis Date = 04/08/16 Pct Recovery = 30% Analysis Date = 04/08/16 Pct Recovery = 30% Analysis Date = 04/04/16 Pct Recovery = 30% Analysis Date = 04/04/16 Pct Recovery = 30% Analysis Date = 03/30/16 Pct Recovery = 30% Analysis Date = 03/30/16 Pct Recovery = 30% Analysis Date = 03/25/16 Pct Recovery = 31% Analysis Date = 03/25/16 Pct Recovery = 31% Analysis Date = 03/21/16 Pct Recovery = 31% Analysis Date = 03/21/16 Pct Recovery = 31% Analysis Date = 03/16/16 Pct Recovery = 31% Analysis Date = 03/16/16 Pct Recovery = 31% Analysis Date = 03/12/16 Pct Recovery = 32% Analysis Date = 03/12/16 Pct Recovery = 32% Analysis Date = 03/07/16 Pct Recovery = 32% Analysis Date = 03/07/16 Pct Recovery = 32% Analysis Date = 03/03/16 Pct Recovery = 32% Analysis Date = 03/03/16 Pct Recovery = 32% Analysis Date = 02/27/16 Pct Recovery = 33% Analysis Date = 02/27/16 Pct Recovery = 33% Analysis Date = 02/22/16 Pct Recovery = 33% Analysis Date = 02/22/16 Pct Recovery = 33% Analysis Date = 02/18/16 Pct Recovery = 33% Analysis Date = 02/18/16 Pct Recovery = 33% Analysis Date = 02/13/16 Pct Recovery = 34% Analysis Date = 02/13/16 Pct Recovery = 34% Analysis Date = 02/09/16 Pct Recovery = 34% Analysis Date = 02/09/16 Pct Recovery = 34% Analysis Date = 02/04/16 Pct Recovery = 34% Analysis Date = 02/04/16 Pct Recovery = 34% Analysis Date = 01/31/16 Pct Recovery = 35% Analysis Date = 01/31/16 Pct Recovery = 35% Analysis Date = 01/26/16 Pct Recovery = 35% Analysis Date = 01/26/16 Pct Recovery = 35% Analysis Date = 01/22/16 Pct Recovery = 35% Analysis Date = 01/22/16 Pct Recovery = 35% Analysis Date = 01/17/16 Pct Recovery = 35% Analysis Date = 01/17/16 Pct Recovery = 35% Analysis Date = 01/12/16 Pct Recovery = 36% Analysis Date = 01/12/16 Pct Recovery = 36% Analysis Date = 01/08/16 Pct Recovery = 36% Analysis Date = 01/08/16 Pct Recovery = 36% Analysis Date = 01/03/16 Pct Recovery = 36% Analysis Date = 01/03/16 Pct Recovery = 36% Analysis Date = 12/30/15 Pct Recovery = 37% Analysis Date = 12/30/15 Pct Recovery = 37% Analysis Date = 12/25/15 Pct Recovery = 37% Analysis Date = 12/25/15 Pct Recovery = 37% Analysis Date = 12/21/15 Pct Recovery = 37% Analysis Date = 12/21/15 Pct Recovery = 37% Analysis Date = 12/16/15 Pct Recovery = 38% Analysis Date = 12/16/15 Pct Recovery = 38% Analysis Date = 12/12/15 Pct Recovery = 38% Analysis Date = 12/12/15 Pct Recovery = 38% Analysis Date = 12/07/15 Pct Recovery = 38% Analysis Date = 12/07/15 Pct Recovery = 38% Analysis Date = 12/02/15 Pct Recovery = 39% Analysis Date = 12/02/15 Pct Recovery = 39% Analysis Date = 11/28/15 Pct Recovery = 39% Analysis Date = 11/28/15 Pct Recovery = 39% Analysis Date = 11/23/15 Pct Recovery = 39% Analysis Date = 11/23/15 Pct Recovery = 39% Analysis Date = 11/19/15 Pct Recovery = 40% Analysis Date = 11/19/15 Pct Recovery = 40% Analysis Date = 11/14/15 Pct Recovery = 40% Analysis Date = 11/14/15 Pct Recovery = 40% Analysis Date = 11/10/15 Pct Recovery = 40% Analysis Date = 11/10/15 Pct Recovery = 40% Analysis Date = 11/05/15 Pct Recovery = 41% Analysis Date = 11/05/15 Pct Recovery = 41% Analysis Date = 10/31/15 Pct Recovery = 41% Analysis Date = 10/31/15 Pct Recovery = 41% Analysis Date = 10/27/15 Pct Recovery = 41% Analysis Date = 10/27/15 Pct Recovery = 41% Analysis Date = 10/22/15 Pct Recovery = 42% Analysis Date = 10/22/15 Pct Recovery = 42% Analysis Date = 10/18/15 Pct Recovery = 42% Analysis Date = 10/18/15 Pct Recovery = 42% Analysis Date = 10/13/15 Pct Recovery = 42% Analysis Date = 10/13/15 Pct Recovery = 42% Analysis Date = 10/09/15 Pct Recovery = 42% Analysis Date = 10/09/15 Pct Recovery = 42% Analysis Date = 10/04/15 Pct Recovery = 43% Analysis Date = 10/04/15 Pct Recovery = 43% Analysis Date = 09/30/15 Pct Recovery = 43% Analysis Date = 09/30/15 Pct Recovery = 43% Analysis Date = 09/25/15 Pct Recovery = 43% Analysis Date = 09/25/15 Pct Recovery = 43% Analysis Date = 09/20/15 Pct Recovery = 44% Analysis Date = 09/20/15 Pct Recovery = 44% Analysis Date = 09/16/15 Pct Recovery = 44% Analysis Date = 09/16/15 Pct Recovery = 44% Analysis Date = 09/11/15 Pct Recovery = 44% Analysis Date = 09/11/15 Pct Recovery = 44% Analysis Date = 09/07/15 Pct Recovery = 45% Analysis Date = 09/07/15 Pct Recovery = 45% Analysis Date = 09/02/15 Pct Recovery = 45% Analysis Date = 09/02/15 Pct Recovery = 45% Analysis Date = 08/29/15 Pct Recovery = 45% Analysis Date = 08/29/15 Pct Recovery = 45% Analysis Date = 08/24/15 Pct Recovery = 46% Analysis Date = 08/24/15 Pct Recovery = 46% Analysis Date = 08/20/15 Pct Recovery = 46% Analysis Date = 08/20/15 Pct Recovery = 46% Analysis Date = 08/15/15 Pct Recovery = 46% Analysis Date = 08/15/15 Pct Recovery = 46% Analysis Date = 08/10/15 Pct Recovery = 47% Analysis Date = 08/10/15 Pct Recovery = 47% Analysis Date = 08/06/15 Pct Recovery = 47% Analysis Date = 08/06/15 Pct Recovery = 47% Analysis Date = 08/01/15 Pct Recovery = 47% Analysis Date = 08/01/15 Pct Recovery = 47% Analysis Date = 07/28/15 Pct Recovery = 48% Analysis Date = 07/28/15 Pct Recovery = 48% Analysis Date = 07/23/15 Pct Recovery = 48% Analysis Date = 07/23/15 Pct Recovery = 48% Analysis Date = 07/19/15 Pct Recovery = 48% Analysis Date = 07/19/15 Pct Recovery = 48% Analysis Date = 07/14/15 Pct Recovery = 49% Analysis Date = 07/14/15 Pct Recovery = 49% Analysis Date = 07/09/15 Pct Recovery = 49% Analysis Date = 07/09/15 Pct Recovery = 49% Analysis Date = 07/05/15 Pct Recovery = 49% Analysis Date = 07/05/15 Pct Recovery = 49% Analysis Date = 06/30/15 Pct Recovery = 49% Analysis Date = 06/30/15 Pct Recovery = 49% Analysis Date = 06/26/15 Pct Recovery = 50% Analysis Date = 06/26/15 Pct Recovery = 50% Analysis Date = 06/21/15 Pct Recovery = 50% Analysis Date = 06/21/15 Pct Recovery = 50% Analysis Date = 06/17/15 Pct Recovery = 50% Analysis Date = 06/17/15 Pct Recovery = 50% Analysis Date = 06/12/15 Pct Recovery = 51% Analysis Date = 06/12/15 Pct Recovery = 51% Analysis Date = 06/08/15 Pct Recovery = 51% Analysis Date = 06/08/15 Pct Recovery = 51% Analysis Date = 06/03/15 Pct Recovery = 51% Analysis Date = 06/03/15 Pct Recovery = 51% Analysis Date = 05/29/15 Pct Recovery = 52% Analysis Date = 05/29/15 Pct Recovery = 52% Analysis Date = 05/25/15 Pct Recovery = 52% Analysis Date = 05/25/15 Pct Recovery = 52% Analysis Date = 05/20/15 Pct Recovery = 52% Analysis Date = 05/20/15 Pct Recovery = 52% Analysis Date = 05/16/15 Pct Recovery = 53% Analysis Date = 05/16/15 Pct Recovery = 53% Analysis Date = 05/11/15 Pct Recovery = 53% Analysis Date = 05/11/15 Pct Recovery = 53% Analysis Date = 05/07/15 Pct Recovery = 53% Analysis Date = 05/07/15 Pct Recovery = 53% Analysis Date = 05/02/15 Pct Recovery = 54% Analysis Date = 05/02/15 Pct Recovery = 54% Analysis Date = 04/28/15 Pct Recovery = 54% Analysis Date = 04/28/15 Pct Recovery = 54% Analysis Date = 04/23/15 Pct Recovery = 53% Analysis Date = 04/23/15 Pct Recovery = 53% Analysis Date = 04/18/15 Pct Recovery = 53% Analysis Date = 04/18/15 Pct Recovery = 53% Analysis Date = 04/14/15 Pct Recovery = 53% Analysis Date = 04/14/15 Pct Recovery = 53% Analysis Date = 04/09/15 Pct Recovery = 52% Analysis Date = 04/09/15 Pct Recovery = 52% Analysis Date = 04/05/15 Pct Recovery = 52% Analysis Date = 04/05/15 Pct Recovery = 52% Analysis Date = 03/31/15 Pct Recovery = 51% Analysis Date = 03/31/15 Pct Recovery = 51% Analysis Date = 03/27/15 Pct Recovery = 51% Analysis Date = 03/27/15 Pct Recovery = 51% Analysis Date = 03/22/15 Pct Recovery = 51% Analysis Date = 03/22/15 Pct Recovery = 51% Analysis Date = 03/17/15 Pct Recovery = 50% Analysis Date = 03/17/15 Pct Recovery = 50% Analysis Date = 03/13/15 Pct Recovery = 50% Analysis Date = 03/13/15 Pct Recovery = 50% Analysis Date = 03/08/15 Pct Recovery = 49% Analysis Date = 03/08/15 Pct Recovery = 49% Analysis Date = 03/04/15 Pct Recovery = 49% Analysis Date = 03/04/15 Pct Recovery = 49% Analysis Date = 02/27/15 Pct Recovery = 48% Analysis Date = 02/27/15 Pct Recovery = 48% Analysis Date = 02/23/15 Pct Recovery = 48% Analysis Date = 02/23/15 Pct Recovery = 48% Analysis Date = 02/18/15 Pct Recovery = 48% Analysis Date = 02/18/15 Pct Recovery = 48% Analysis Date = 02/14/15 Pct Recovery = 47% Analysis Date = 02/14/15 Pct Recovery = 47% Analysis Date = 02/09/15 Pct Recovery = 47% Analysis Date = 02/09/15 Pct Recovery = 47% Analysis Date = 02/04/15 Pct Recovery = 46% Analysis Date = 02/04/15 Pct Recovery = 46% Analysis Date = 01/31/15 Pct Recovery = 46% Analysis Date = 01/31/15 Pct Recovery = 46% Analysis Date = 01/26/15 Pct Recovery = 46% Analysis Date = 01/26/15 Pct Recovery = 46% Analysis Date = 01/22/15 Pct Recovery = 45% Analysis Date = 01/22/15 Pct Recovery = 45% Analysis Date = 01/17/15 Pct Recovery = 45% Analysis Date = 01/17/15 Pct Recovery = 45% Analysis Date = 01/13/15 Pct Recovery = 44% Analysis Date = 01/13/15 Pct Recovery = 44% Analysis Date = 01/08/15 Pct Recovery = 44% Analysis Date = 01/08/15 Pct Recovery = 44% Analysis Date = 01/04/15 Pct Recovery = 44% Analysis Date = 01/04/15 Pct Recovery = 44% Analysis Date = 12/30/14 Pct Recovery = 43% Analysis Date = 12/30/14 Pct Recovery = 43% Analysis Date = 12/25/14 Pct Recovery = 43% Analysis Date = 12/25/14 Pct Recovery = 43% Analysis Date = 12/21/14 Pct Recovery = 42% Analysis Date = 12/21/14 Pct Recovery = 42% Analysis Date = 12/16/14 Pct Recovery = 42% Analysis Date = 12/16/14 Pct Recovery = 42% Analysis Date = 12/12/14 Pct Recovery = 41% Analysis Date = 12/12/14 Pct Recovery = 41% Analysis Date = 12/07/14 Pct Recovery = 41% Analysis Date = 12/07/14 Pct Recovery = 41% Analysis Date = 12/03/14 Pct Recovery = 41% Analysis Date = 12/03/14 Pct Recovery = 41% Analysis Date = 11/28/14 Pct Recovery = 41% Analysis Date = 11/28/14 Pct Recovery = 41% Analysis Date = 11/23/14 Pct Recovery = 41% Analysis Date = 11/23/14 Pct Recovery = 41% Analysis Date = 11/19/14 Pct Recovery = 40% Analysis Date = 11/19/14 Pct Recovery = 40% Analysis Date = 11/14/14 Pct Recovery = 40% Analysis Date = 11/14/14 Pct Recovery = 40% Analysis Date = 11/10/14 Pct Recovery = 40% Analysis Date = 11/10/14 Pct Recovery = 40% Analysis Date = 11/05/14 Pct Recovery = 40% Analysis Date = 11/05/14 Pct Recovery = 40% Analysis Date = 11/01/14 Pct Recovery = 40% Analysis Date = 11/01/14 Pct Recovery = 40% Analysis Date = 10/27/14 Pct Recovery = 40% Analysis Date = 10/27/14 Pct Recovery = 40% Analysis Date = 10/23/14 Pct Recovery = 40% Analysis Date = 10/23/14 Pct Recovery = 40% Analysis Date = 10/18/14 Pct Recovery = 39% Analysis Date = 10/18/14 Pct Recovery = 39% Analysis Date = 10/13/14 Pct Recovery = 39% Analysis Date = 10/13/14 Pct Recovery = 39% Analysis Date = 10/09/14 Pct Recovery = 39% Analysis Date = 10/09/14 Pct Recovery = 39% Analysis Date = 10/04/14 Pct Recovery = 40% Analysis Date = 10/04/14 Pct Recovery = 40% Analysis Date = 09/30/14 Pct Recovery = 40% Analysis Date = 09/30/14 Pct Recovery = 40% Analysis Date = 09/25/14 Pct Recovery = 40% Analysis Date = 09/25/14 Pct Recovery = 40% Analysis Date = 09/21/14 Pct Recovery = 40% Analysis Date = 09/21/14 Pct Recovery = 40% Analysis Date = 09/16/14 Pct Recovery = 41% Analysis Date = 09/16/14 Pct Recovery = 41% Analysis Date = 09/12/14 Pct Recovery = 41% Analysis Date = 09/12/14 Pct Recovery = 41% Analysis Date = 09/07/14 Pct Recovery = 41% Analysis Date = 09/07/14 Pct Recovery = 41% Analysis Date = 09/02/14 Pct Recovery = 41% Analysis Date = 09/02/14 Pct Recovery = 41% Analysis Date = 08/29/14 Pct Recovery = 42% Analysis Date = 08/29/14 Pct Recovery = 42% Analysis Date = 08/24/14 Pct Recovery = 42% Analysis Date = 08/24/14 Pct Recovery = 42% Analysis Date = 08/20/14 Pct Recovery = 43% Analysis Date = 08/20/14 Pct Recovery = 43% Analysis Date = 08/15/14 Pct Recovery = 43% Analysis Date = 08/15/14 Pct Recovery = 43% Analysis Date = 08/11/14 Pct Recovery = 44% Analysis Date = 08/11/14 Pct Recovery = 44% Analysis Date = 08/06/14 Pct Recovery = 44% Analysis Date = 08/06/14 Pct Recovery = 44% Analysis Date = 08/01/14 Pct Recovery = 45% Analysis Date = 08/01/14 Pct Recovery = 45% Analysis Date = 07/28/14 Pct Recovery = 45% Analysis Date = 07/28/14 Pct Recovery = 45% Analysis Date = 07/23/14 Pct Recovery = 46% Analysis Date = 07/23/14 Pct Recovery = 46% Analysis Date = 07/19/14 Pct Recovery = 46% Analysis Date = 07/19/14 Pct Recovery = 46% Analysis Date = 07/14/14 Pct Recovery = 47% Analysis Date = 07/14/14 Pct Recovery = 47% Analysis Date = 07/10/14 Pct Recovery = 47% Analysis Date = 07/10/14 Pct Recovery = 47% Analysis Date = 07/05/14 Pct Recovery = 48% Analysis Date = 07/05/14 Pct Recovery = 48% Analysis Date = 07/01/14 Pct Recovery = 48% Analysis Date = 07/01/14 Pct Recovery = 48% Analysis Date = 06/26/14 Pct Recovery = 49% Analysis Date = 06/26/14 Pct Recovery = 49% Analysis Date = 06/21/14 Pct Recovery = 49% Analysis Date = 06/21/14 Pct Recovery = 49% Analysis Date = 06/17/14 Pct Recovery = 49% Analysis Date = 06/17/14 Pct Recovery = 49% Analysis Date = 06/12/14 Pct Recovery = 50% Analysis Date = 06/12/14 Pct Recovery = 50% Analysis Date = 06/08/14 Pct Recovery = 50% Analysis Date = 06/08/14 Pct Recovery = 50% Analysis Date = 06/03/14 Pct Recovery = 51% Analysis Date = 06/03/14 Pct Recovery = 51% Analysis Date = 05/30/14 Pct Recovery = 51% Analysis Date = 05/30/14 Pct Recovery = 51% Analysis Date = 05/25/14 Pct Recovery = 52% Analysis Date = 05/25/14 Pct Recovery = 52% Analysis Date = 05/21/14 Pct Recovery = 52% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
ERYTHROMYCIN

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 31 37% 18% 37% 24%
Total 31 37% 18% 37% 24%

Sample Statistics
ERYTHROMYCIN

Characteristic N % % Basis
Plotted 31 40% Spiked
Estimated Values 10 13% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 8 10% Spiked
Spiked 77 .  
False Negatives 38 49% 38 out of 77
Not Spiked 38 .  
False Positives 0 0% 0 out of 38

BQS OBSP Determination:
EZETIMIBE
METHOD: 2440 , TESTIDCODE: 67487LCM56
Open Data Set

Analysis Date = 06/09/15 SpikeMix = Abs 051315: 20 µl & Abs 050115: 20 µl Pct Recovery = 266% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 57% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 86% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 58% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 62% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 80 µl & ERA 0406-15-08: 80 µl Pct Recovery = 28% Analysis Date = 11/24/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 85% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 80 µl & Abs 051315: 80 µl Pct Recovery = 131% Analysis Date = 10/01/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 77% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 49% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 66% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 84% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 86% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 30% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 24% Analysis Date = 09/24/16 SpikeMix = Crescent EN160610015: 80 µl & Abs 061416: 80 µl Pct Recovery = 43% Analysis Date = 09/24/16 SpikeMix = Abs 061416: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 37% Analysis Date = 03/11/15 SpikeMix = ERA 0318-14-02: 15 µl & Abs 041714: 15 µl Pct Recovery = 85% Analysis Date = 02/06/15 SpikeMix = Abs 041814: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 39% Analysis Date = 12/06/14 SpikeMix = ERA 0318-14-02: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 19% Analysis Date = 10/11/14 SpikeMix = ERA 0318-14-02: 60 µl & ERA 0319-14-04: 60 µl Pct Recovery = 22% Analysis Date = 12/07/14 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 42% Analysis Date = 10/25/14 SpikeMix = Abs 041614: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 51% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 65% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-08: 40 µl & ERA 0406-15-09: 40 µl Pct Recovery = 36% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 99% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 70% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-07A: 40 µl & Abs 051315: 40 µl Pct Recovery = 60% Analysis Date = 07/31/15 SpikeMix = Abs 051315: 40 µl & Abs 052215: 40 µl Pct Recovery = 18% Analysis Date = 07/30/15 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 24% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 26% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 47% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 49% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 45% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 37% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 67% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 77% Analysis Date = 12/07/14 SpikeMix = ERA 0318-14-02: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 34% Analysis Date = 11/04/14 SpikeMix = Abs 041814: 8 µl & ERA 0318-14-02: 8 µl Pct Recovery = 38% Analysis Date = 04/30/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 81% Analysis Date = 10/24/14 SpikeMix = ERA 0319-14-05: 8 µl & Abs 041614: 8 µl Pct Recovery = 39% Analysis Date = 05/17/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 67% Analysis Date = 04/23/14 SpikeMix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.2: 20 µl Pct Recovery = 44% Analysis Date = 04/27/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 80% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 67% Analysis Date = 11/25/15 SpikeMix = Abs 050115: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 30% Analysis Date = 02/23/16 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 37% Analysis Date = 06/26/15 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 124% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 66% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 61% Analysis Date = 01/18/17 Pct Recovery = 51% Analysis Date = 01/13/17 Pct Recovery = 52% Analysis Date = 01/13/17 Pct Recovery = 52% Analysis Date = 01/08/17 Pct Recovery = 52% Analysis Date = 01/08/17 Pct Recovery = 52% Analysis Date = 01/03/17 Pct Recovery = 52% Analysis Date = 01/03/17 Pct Recovery = 52% Analysis Date = 12/29/16 Pct Recovery = 52% Analysis Date = 12/29/16 Pct Recovery = 52% Analysis Date = 12/24/16 Pct Recovery = 52% Analysis Date = 12/24/16 Pct Recovery = 52% Analysis Date = 12/19/16 Pct Recovery = 53% Analysis Date = 12/19/16 Pct Recovery = 53% Analysis Date = 12/14/16 Pct Recovery = 53% Analysis Date = 12/14/16 Pct Recovery = 53% Analysis Date = 12/09/16 Pct Recovery = 53% Analysis Date = 12/09/16 Pct Recovery = 53% Analysis Date = 12/04/16 Pct Recovery = 53% Analysis Date = 12/04/16 Pct Recovery = 53% Analysis Date = 11/29/16 Pct Recovery = 53% Analysis Date = 11/29/16 Pct Recovery = 53% Analysis Date = 11/24/16 Pct Recovery = 54% Analysis Date = 11/24/16 Pct Recovery = 54% Analysis Date = 11/19/16 Pct Recovery = 54% Analysis Date = 11/19/16 Pct Recovery = 54% Analysis Date = 11/14/16 Pct Recovery = 54% Analysis Date = 11/14/16 Pct Recovery = 54% Analysis Date = 11/09/16 Pct Recovery = 54% Analysis Date = 11/09/16 Pct Recovery = 54% Analysis Date = 11/04/16 Pct Recovery = 54% Analysis Date = 11/04/16 Pct Recovery = 54% Analysis Date = 10/30/16 Pct Recovery = 54% Analysis Date = 10/30/16 Pct Recovery = 54% Analysis Date = 10/25/16 Pct Recovery = 55% Analysis Date = 10/25/16 Pct Recovery = 55% Analysis Date = 10/20/16 Pct Recovery = 55% Analysis Date = 10/20/16 Pct Recovery = 55% Analysis Date = 10/15/16 Pct Recovery = 55% Analysis Date = 10/15/16 Pct Recovery = 55% Analysis Date = 10/10/16 Pct Recovery = 55% Analysis Date = 10/10/16 Pct Recovery = 55% Analysis Date = 10/05/16 Pct Recovery = 56% Analysis Date = 10/05/16 Pct Recovery = 56% Analysis Date = 09/30/16 Pct Recovery = 56% Analysis Date = 09/30/16 Pct Recovery = 56% Analysis Date = 09/25/16 Pct Recovery = 56% Analysis Date = 09/25/16 Pct Recovery = 56% Analysis Date = 09/20/16 Pct Recovery = 56% Analysis Date = 09/20/16 Pct Recovery = 56% Analysis Date = 09/15/16 Pct Recovery = 56% Analysis Date = 09/15/16 Pct Recovery = 56% Analysis Date = 09/10/16 Pct Recovery = 57% Analysis Date = 09/10/16 Pct Recovery = 57% Analysis Date = 09/05/16 Pct Recovery = 57% Analysis Date = 09/05/16 Pct Recovery = 57% Analysis Date = 08/31/16 Pct Recovery = 57% Analysis Date = 08/31/16 Pct Recovery = 57% Analysis Date = 08/26/16 Pct Recovery = 57% Analysis Date = 08/26/16 Pct Recovery = 57% Analysis Date = 08/21/16 Pct Recovery = 58% Analysis Date = 08/21/16 Pct Recovery = 58% Analysis Date = 08/16/16 Pct Recovery = 58% Analysis Date = 08/16/16 Pct Recovery = 58% Analysis Date = 08/11/16 Pct Recovery = 58% Analysis Date = 08/11/16 Pct Recovery = 58% Analysis Date = 08/06/16 Pct Recovery = 58% Analysis Date = 08/06/16 Pct Recovery = 58% Analysis Date = 08/01/16 Pct Recovery = 58% Analysis Date = 08/01/16 Pct Recovery = 58% Analysis Date = 07/27/16 Pct Recovery = 59% Analysis Date = 07/27/16 Pct Recovery = 59% Analysis Date = 07/22/16 Pct Recovery = 59% Analysis Date = 07/22/16 Pct Recovery = 59% Analysis Date = 07/17/16 Pct Recovery = 59% Analysis Date = 07/17/16 Pct Recovery = 59% Analysis Date = 07/12/16 Pct Recovery = 59% Analysis Date = 07/12/16 Pct Recovery = 59% Analysis Date = 07/07/16 Pct Recovery = 59% Analysis Date = 07/07/16 Pct Recovery = 59% Analysis Date = 07/02/16 Pct Recovery = 59% Analysis Date = 07/02/16 Pct Recovery = 59% Analysis Date = 06/27/16 Pct Recovery = 59% Analysis Date = 06/27/16 Pct Recovery = 59% Analysis Date = 06/22/16 Pct Recovery = 60% Analysis Date = 06/22/16 Pct Recovery = 60% Analysis Date = 06/17/16 Pct Recovery = 60% Analysis Date = 06/17/16 Pct Recovery = 60% Analysis Date = 06/12/16 Pct Recovery = 60% Analysis Date = 06/12/16 Pct Recovery = 60% Analysis Date = 06/07/16 Pct Recovery = 60% Analysis Date = 06/07/16 Pct Recovery = 60% Analysis Date = 06/02/16 Pct Recovery = 60% Analysis Date = 06/02/16 Pct Recovery = 60% Analysis Date = 05/28/16 Pct Recovery = 60% Analysis Date = 05/28/16 Pct Recovery = 60% Analysis Date = 05/23/16 Pct Recovery = 60% Analysis Date = 05/23/16 Pct Recovery = 60% Analysis Date = 05/18/16 Pct Recovery = 61% Analysis Date = 05/18/16 Pct Recovery = 61% Analysis Date = 05/13/16 Pct Recovery = 61% Analysis Date = 05/13/16 Pct Recovery = 61% Analysis Date = 05/08/16 Pct Recovery = 61% Analysis Date = 05/08/16 Pct Recovery = 61% Analysis Date = 05/03/16 Pct Recovery = 61% Analysis Date = 05/03/16 Pct Recovery = 61% Analysis Date = 04/28/16 Pct Recovery = 61% Analysis Date = 04/28/16 Pct Recovery = 61% Analysis Date = 04/23/16 Pct Recovery = 61% Analysis Date = 04/23/16 Pct Recovery = 61% Analysis Date = 04/18/16 Pct Recovery = 62% Analysis Date = 04/18/16 Pct Recovery = 62% Analysis Date = 04/13/16 Pct Recovery = 62% Analysis Date = 04/13/16 Pct Recovery = 62% Analysis Date = 04/08/16 Pct Recovery = 62% Analysis Date = 04/08/16 Pct Recovery = 62% Analysis Date = 04/03/16 Pct Recovery = 62% Analysis Date = 04/03/16 Pct Recovery = 62% Analysis Date = 03/29/16 Pct Recovery = 62% Analysis Date = 03/29/16 Pct Recovery = 62% Analysis Date = 03/24/16 Pct Recovery = 62% Analysis Date = 03/24/16 Pct Recovery = 62% Analysis Date = 03/19/16 Pct Recovery = 63% Analysis Date = 03/19/16 Pct Recovery = 63% Analysis Date = 03/14/16 Pct Recovery = 63% Analysis Date = 03/14/16 Pct Recovery = 63% Analysis Date = 03/09/16 Pct Recovery = 63% Analysis Date = 03/09/16 Pct Recovery = 63% Analysis Date = 03/04/16 Pct Recovery = 63% Analysis Date = 03/04/16 Pct Recovery = 63% Analysis Date = 02/28/16 Pct Recovery = 63% Analysis Date = 02/28/16 Pct Recovery = 63% Analysis Date = 02/23/16 Pct Recovery = 63% Analysis Date = 02/23/16 Pct Recovery = 63% Analysis Date = 02/18/16 Pct Recovery = 64% Analysis Date = 02/18/16 Pct Recovery = 64% Analysis Date = 02/13/16 Pct Recovery = 64% Analysis Date = 02/13/16 Pct Recovery = 64% Analysis Date = 02/08/16 Pct Recovery = 65% Analysis Date = 02/08/16 Pct Recovery = 65% Analysis Date = 02/03/16 Pct Recovery = 65% Analysis Date = 02/03/16 Pct Recovery = 65% Analysis Date = 01/29/16 Pct Recovery = 66% Analysis Date = 01/29/16 Pct Recovery = 66% Analysis Date = 01/24/16 Pct Recovery = 66% Analysis Date = 01/24/16 Pct Recovery = 66% Analysis Date = 01/19/16 Pct Recovery = 67% Analysis Date = 01/19/16 Pct Recovery = 67% Analysis Date = 01/14/16 Pct Recovery = 67% Analysis Date = 01/14/16 Pct Recovery = 67% Analysis Date = 01/09/16 Pct Recovery = 68% Analysis Date = 01/09/16 Pct Recovery = 68% Analysis Date = 01/04/16 Pct Recovery = 68% Analysis Date = 01/04/16 Pct Recovery = 68% Analysis Date = 12/30/15 Pct Recovery = 69% Analysis Date = 12/30/15 Pct Recovery = 69% Analysis Date = 12/25/15 Pct Recovery = 69% Analysis Date = 12/25/15 Pct Recovery = 69% Analysis Date = 12/20/15 Pct Recovery = 70% Analysis Date = 12/20/15 Pct Recovery = 70% Analysis Date = 12/15/15 Pct Recovery = 70% Analysis Date = 12/15/15 Pct Recovery = 70% Analysis Date = 12/10/15 Pct Recovery = 71% Analysis Date = 12/10/15 Pct Recovery = 71% Analysis Date = 12/05/15 Pct Recovery = 71% Analysis Date = 12/05/15 Pct Recovery = 71% Analysis Date = 11/30/15 Pct Recovery = 72% Analysis Date = 11/30/15 Pct Recovery = 72% Analysis Date = 11/25/15 Pct Recovery = 72% Analysis Date = 11/25/15 Pct Recovery = 72% Analysis Date = 11/20/15 Pct Recovery = 73% Analysis Date = 11/20/15 Pct Recovery = 73% Analysis Date = 11/15/15 Pct Recovery = 73% Analysis Date = 11/15/15 Pct Recovery = 73% Analysis Date = 11/10/15 Pct Recovery = 74% Analysis Date = 11/10/15 Pct Recovery = 74% Analysis Date = 11/05/15 Pct Recovery = 74% Analysis Date = 11/05/15 Pct Recovery = 74% Analysis Date = 10/31/15 Pct Recovery = 75% Analysis Date = 10/31/15 Pct Recovery = 75% Analysis Date = 10/26/15 Pct Recovery = 75% Analysis Date = 10/26/15 Pct Recovery = 75% Analysis Date = 10/21/15 Pct Recovery = 76% Analysis Date = 10/21/15 Pct Recovery = 76% Analysis Date = 10/16/15 Pct Recovery = 76% Analysis Date = 10/16/15 Pct Recovery = 76% Analysis Date = 10/11/15 Pct Recovery = 77% Analysis Date = 10/11/15 Pct Recovery = 77% Analysis Date = 10/06/15 Pct Recovery = 77% Analysis Date = 10/06/15 Pct Recovery = 77% Analysis Date = 10/01/15 Pct Recovery = 78% Analysis Date = 10/01/15 Pct Recovery = 78% Analysis Date = 09/26/15 Pct Recovery = 77% Analysis Date = 09/26/15 Pct Recovery = 77% Analysis Date = 09/21/15 Pct Recovery = 77% Analysis Date = 09/21/15 Pct Recovery = 77% Analysis Date = 09/16/15 Pct Recovery = 76% Analysis Date = 09/16/15 Pct Recovery = 76% Analysis Date = 09/11/15 Pct Recovery = 76% Analysis Date = 09/11/15 Pct Recovery = 76% Analysis Date = 09/05/15 Pct Recovery = 75% Analysis Date = 09/05/15 Pct Recovery = 75% Analysis Date = 08/31/15 Pct Recovery = 75% Analysis Date = 08/31/15 Pct Recovery = 75% Analysis Date = 08/26/15 Pct Recovery = 75% Analysis Date = 08/26/15 Pct Recovery = 75% Analysis Date = 08/21/15 Pct Recovery = 74% Analysis Date = 08/21/15 Pct Recovery = 74% Analysis Date = 08/16/15 Pct Recovery = 74% Analysis Date = 08/16/15 Pct Recovery = 74% Analysis Date = 08/11/15 Pct Recovery = 73% Analysis Date = 08/11/15 Pct Recovery = 73% Analysis Date = 08/06/15 Pct Recovery = 73% Analysis Date = 08/06/15 Pct Recovery = 73% Analysis Date = 08/01/15 Pct Recovery = 72% Analysis Date = 08/01/15 Pct Recovery = 72% Analysis Date = 07/27/15 Pct Recovery = 72% Analysis Date = 07/27/15 Pct Recovery = 72% Analysis Date = 07/22/15 Pct Recovery = 72% Analysis Date = 07/22/15 Pct Recovery = 72% Analysis Date = 07/17/15 Pct Recovery = 71% Analysis Date = 07/17/15 Pct Recovery = 71% Analysis Date = 07/12/15 Pct Recovery = 71% Analysis Date = 07/12/15 Pct Recovery = 71% Analysis Date = 07/07/15 Pct Recovery = 70% Analysis Date = 07/07/15 Pct Recovery = 70% Analysis Date = 07/02/15 Pct Recovery = 70% Analysis Date = 07/02/15 Pct Recovery = 70% Analysis Date = 06/27/15 Pct Recovery = 69% Analysis Date = 06/27/15 Pct Recovery = 69% Analysis Date = 06/22/15 Pct Recovery = 69% Analysis Date = 06/22/15 Pct Recovery = 69% Analysis Date = 06/17/15 Pct Recovery = 68% Analysis Date = 06/17/15 Pct Recovery = 68% Analysis Date = 06/12/15 Pct Recovery = 68% Analysis Date = 06/12/15 Pct Recovery = 68% Analysis Date = 06/07/15 Pct Recovery = 68% Analysis Date = 06/07/15 Pct Recovery = 68% Analysis Date = 06/02/15 Pct Recovery = 67% Analysis Date = 06/02/15 Pct Recovery = 67% Analysis Date = 05/28/15 Pct Recovery = 67% Analysis Date = 05/28/15 Pct Recovery = 67% Analysis Date = 05/23/15 Pct Recovery = 67% Analysis Date = 05/23/15 Pct Recovery = 67% Analysis Date = 05/18/15 Pct Recovery = 66% Analysis Date = 05/18/15 Pct Recovery = 66% Analysis Date = 05/13/15 Pct Recovery = 66% Analysis Date = 05/13/15 Pct Recovery = 66% Analysis Date = 05/08/15 Pct Recovery = 66% Analysis Date = 05/08/15 Pct Recovery = 66% Analysis Date = 05/03/15 Pct Recovery = 65% Analysis Date = 05/03/15 Pct Recovery = 65% Analysis Date = 04/28/15 Pct Recovery = 65% Analysis Date = 04/28/15 Pct Recovery = 65% Analysis Date = 04/23/15 Pct Recovery = 65% Analysis Date = 04/23/15 Pct Recovery = 65% Analysis Date = 04/18/15 Pct Recovery = 64% Analysis Date = 04/18/15 Pct Recovery = 64% Analysis Date = 04/13/15 Pct Recovery = 64% Analysis Date = 04/13/15 Pct Recovery = 64% Analysis Date = 04/08/15 Pct Recovery = 64% Analysis Date = 04/08/15 Pct Recovery = 64% Analysis Date = 04/03/15 Pct Recovery = 63% Analysis Date = 04/03/15 Pct Recovery = 63% Analysis Date = 03/29/15 Pct Recovery = 63% Analysis Date = 03/29/15 Pct Recovery = 63% Analysis Date = 03/24/15 Pct Recovery = 63% Analysis Date = 03/24/15 Pct Recovery = 63% Analysis Date = 03/19/15 Pct Recovery = 62% Analysis Date = 03/19/15 Pct Recovery = 62% Analysis Date = 03/14/15 Pct Recovery = 62% Analysis Date = 03/14/15 Pct Recovery = 62% Analysis Date = 03/09/15 Pct Recovery = 62% Analysis Date = 03/09/15 Pct Recovery = 62% Analysis Date = 03/04/15 Pct Recovery = 61% Analysis Date = 03/04/15 Pct Recovery = 61% Analysis Date = 02/27/15 Pct Recovery = 61% Analysis Date = 02/27/15 Pct Recovery = 61% Analysis Date = 02/22/15 Pct Recovery = 61% Analysis Date = 02/22/15 Pct Recovery = 61% Analysis Date = 02/17/15 Pct Recovery = 60% Analysis Date = 02/17/15 Pct Recovery = 60% Analysis Date = 02/12/15 Pct Recovery = 60% Analysis Date = 02/12/15 Pct Recovery = 60% Analysis Date = 02/07/15 Pct Recovery = 60% Analysis Date = 02/07/15 Pct Recovery = 60% Analysis Date = 02/02/15 Pct Recovery = 59% Analysis Date = 02/02/15 Pct Recovery = 59% Analysis Date = 01/28/15 Pct Recovery = 59% Analysis Date = 01/28/15 Pct Recovery = 59% Analysis Date = 01/23/15 Pct Recovery = 59% Analysis Date = 01/23/15 Pct Recovery = 59% Analysis Date = 01/18/15 Pct Recovery = 58% Analysis Date = 01/18/15 Pct Recovery = 58% Analysis Date = 01/13/15 Pct Recovery = 58% Analysis Date = 01/13/15 Pct Recovery = 58% Analysis Date = 01/08/15 Pct Recovery = 58% Analysis Date = 01/08/15 Pct Recovery = 58% Analysis Date = 01/03/15 Pct Recovery = 57% Analysis Date = 01/03/15 Pct Recovery = 57% Analysis Date = 12/29/14 Pct Recovery = 57% Analysis Date = 12/29/14 Pct Recovery = 57% Analysis Date = 12/24/14 Pct Recovery = 57% Analysis Date = 12/24/14 Pct Recovery = 57% Analysis Date = 12/19/14 Pct Recovery = 56% Analysis Date = 12/19/14 Pct Recovery = 56% Analysis Date = 12/14/14 Pct Recovery = 56% Analysis Date = 12/14/14 Pct Recovery = 56% Analysis Date = 12/09/14 Pct Recovery = 56% Analysis Date = 12/09/14 Pct Recovery = 56% Analysis Date = 12/04/14 Pct Recovery = 55% Analysis Date = 12/04/14 Pct Recovery = 55% Analysis Date = 11/29/14 Pct Recovery = 55% Analysis Date = 11/29/14 Pct Recovery = 55% Analysis Date = 11/24/14 Pct Recovery = 55% Analysis Date = 11/24/14 Pct Recovery = 55% Analysis Date = 11/19/14 Pct Recovery = 54% Analysis Date = 11/19/14 Pct Recovery = 54% Analysis Date = 11/14/14 Pct Recovery = 54% Analysis Date = 11/14/14 Pct Recovery = 54% Analysis Date = 11/09/14 Pct Recovery = 54% Analysis Date = 11/09/14 Pct Recovery = 54% Analysis Date = 11/04/14 Pct Recovery = 53% Analysis Date = 11/04/14 Pct Recovery = 53% Analysis Date = 10/30/14 Pct Recovery = 53% Analysis Date = 10/30/14 Pct Recovery = 53% Analysis Date = 10/25/14 Pct Recovery = 52% Analysis Date = 10/25/14 Pct Recovery = 52% Analysis Date = 10/20/14 Pct Recovery = 52% Analysis Date = 10/20/14 Pct Recovery = 52% Analysis Date = 10/15/14 Pct Recovery = 52% Analysis Date = 10/15/14 Pct Recovery = 52% Analysis Date = 10/10/14 Pct Recovery = 51% Analysis Date = 10/10/14 Pct Recovery = 51% Analysis Date = 10/05/14 Pct Recovery = 51% Analysis Date = 10/05/14 Pct Recovery = 51% Analysis Date = 09/30/14 Pct Recovery = 50% Analysis Date = 09/30/14 Pct Recovery = 50% Analysis Date = 09/25/14 Pct Recovery = 50% Analysis Date = 09/25/14 Pct Recovery = 50% Analysis Date = 09/20/14 Pct Recovery = 49% Analysis Date = 09/20/14 Pct Recovery = 49% Analysis Date = 09/15/14 Pct Recovery = 49% Analysis Date = 09/15/14 Pct Recovery = 49% Analysis Date = 09/10/14 Pct Recovery = 48% Analysis Date = 09/10/14 Pct Recovery = 48% Analysis Date = 09/05/14 Pct Recovery = 48% Analysis Date = 09/05/14 Pct Recovery = 48% Analysis Date = 08/31/14 Pct Recovery = 48% Analysis Date = 08/31/14 Pct Recovery = 48% Analysis Date = 08/26/14 Pct Recovery = 47% Analysis Date = 08/26/14 Pct Recovery = 47% Analysis Date = 08/21/14 Pct Recovery = 47% Analysis Date = 08/21/14 Pct Recovery = 47% Analysis Date = 08/16/14 Pct Recovery = 46% Analysis Date = 08/16/14 Pct Recovery = 46% Analysis Date = 08/11/14 Pct Recovery = 46% Analysis Date = 08/11/14 Pct Recovery = 46% Analysis Date = 08/06/14 Pct Recovery = 45% Analysis Date = 08/06/14 Pct Recovery = 45% Analysis Date = 08/01/14 Pct Recovery = 45% Analysis Date = 08/01/14 Pct Recovery = 45% Analysis Date = 07/27/14 Pct Recovery = 44% Analysis Date = 07/27/14 Pct Recovery = 44% Analysis Date = 07/22/14 Pct Recovery = 44% Analysis Date = 07/22/14 Pct Recovery = 44% Analysis Date = 07/17/14 Pct Recovery = 44% Analysis Date = 07/17/14 Pct Recovery = 44% Analysis Date = 07/12/14 Pct Recovery = 43% Analysis Date = 07/12/14 Pct Recovery = 43% Analysis Date = 07/07/14 Pct Recovery = 43% Analysis Date = 07/07/14 Pct Recovery = 43% Analysis Date = 07/02/14 Pct Recovery = 42% Analysis Date = 07/02/14 Pct Recovery = 42% Analysis Date = 06/27/14 Pct Recovery = 42% Analysis Date = 06/27/14 Pct Recovery = 42% Analysis Date = 06/22/14 Pct Recovery = 41% Analysis Date = 06/22/14 Pct Recovery = 41% Analysis Date = 06/17/14 Pct Recovery = 41% Analysis Date = 06/17/14 Pct Recovery = 41% Analysis Date = 06/12/14 Pct Recovery = 40% Analysis Date = 06/12/14 Pct Recovery = 40% Analysis Date = 06/07/14 Pct Recovery = 40% Analysis Date = 06/07/14 Pct Recovery = 40% Analysis Date = 06/02/14 Pct Recovery = 40% Analysis Date = 06/02/14 Pct Recovery = 40% Analysis Date = 05/28/14 Pct Recovery = 39% Analysis Date = 05/28/14 Pct Recovery = 39% Analysis Date = 05/23/14 Pct Recovery = 39% Analysis Date = 05/23/14 Pct Recovery = 39% Analysis Date = 05/18/14 Pct Recovery = 38% Analysis Date = 05/18/14 Pct Recovery = 38% Analysis Date = 05/13/14 Pct Recovery = 38% Analysis Date = 05/13/14 Pct Recovery = 38% Analysis Date = 05/08/14 Pct Recovery = 37% Analysis Date = 05/08/14 Pct Recovery = 37% Analysis Date = 05/03/14 Pct Recovery = 37% Analysis Date = 05/03/14 Pct Recovery = 37% Analysis Date = 04/28/14 Pct Recovery = 36% Analysis Date = 04/28/14 Pct Recovery = 36% Analysis Date = 04/23/14 Pct Recovery = 36% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
EZETIMIBE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 2 63% 3% 63% 4%
>= Reporting Level 48 60% 40% 50% 30%
Total 50 60% 39% 54% 30%

Sample Statistics
EZETIMIBE

Characteristic N % % Basis
Plotted 50 66% Spiked
Estimated Values 50 66% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 10 13% Spiked
Spiked 76 .  
False Negatives 16 21% 16 out of 76
Not Spiked 39 .  
False Positives 0 0% 0 out of 39

BQS OBSP Determination:
FADROZOLE
METHOD: 2440 , TESTIDCODE: 68012LCM56
Open Data Set

Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 51% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 51% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 80 µl & ERA 0406-15-08: 80 µl Pct Recovery = 74% Analysis Date = 11/04/15 SpikeMix = Abs 052215: 80 µl & Abs 050115: 80 µl Pct Recovery = 68% Analysis Date = 01/17/16 SpikeMix = ERA 0406-15-09: 80 µl & ERA 0406-15-07A: 80 µl Pct Recovery = 58% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 80 µl & Abs 051315: 80 µl Pct Recovery = 64% Analysis Date = 11/18/16 SpikeMix = ERA 04281604: 80 µl & ERA 04281603: 80 µl Pct Recovery = 52% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & ERA 04281604: 80 µl Pct Recovery = 54% Analysis Date = 09/24/16 SpikeMix = Crescent EN160610015: 80 µl & Abs 061416: 80 µl Pct Recovery = 59% Analysis Date = 09/24/16 SpikeMix = Abs 061416: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 56% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 61% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 64% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 61% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 56% Analysis Date = 04/29/15 SpikeMix = ERA 0319-14-05: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 106% Analysis Date = 03/11/15 SpikeMix = ERA 0318-14-02: 15 µl & Abs 041714: 15 µl Pct Recovery = 66% Analysis Date = 02/06/15 SpikeMix = Abs 041814: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 72% Analysis Date = 12/06/14 SpikeMix = ERA 0318-14-02: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 66% Analysis Date = 10/11/14 SpikeMix = ERA 0318-14-02: 60 µl & ERA 0319-14-04: 60 µl Pct Recovery = 64% Analysis Date = 08/21/14 SpikeMix = ERA 0318-14-02: 60 µl & Abs 041714: 60 µl Pct Recovery = 65% Analysis Date = 07/26/14 SpikeMix = ERA 0319-14-05: 60 µl & ERA 0318-14-02: 60 µl Pct Recovery = 86% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 72% Analysis Date = 12/07/14 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 64% Analysis Date = 10/25/14 SpikeMix = Abs 041614: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 68% Analysis Date = 06/22/14 SpikeMix = Abs 041814: 60 µl & Abs 041614: 60 µl Pct Recovery = 75% Analysis Date = 06/11/14 SpikeMix = Abs 041614: 60 µl & Abs 041714: 60 µl Pct Recovery = 67% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 62% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 53% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 68% Analysis Date = 02/23/16 SpikeMix = Abs 052215: 40 µl & Abs 050115: 40 µl Pct Recovery = 74% Analysis Date = 07/31/15 SpikeMix = ERA 0406-15-09: 40 µl & Abs 050115: 40 µl Pct Recovery = 73% Analysis Date = 07/30/15 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 67% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-07A: 40 µl & Abs 051315: 40 µl Pct Recovery = 46% Analysis Date = 11/04/15 SpikeMix = ERA 0406-15-07A: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 58% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 63% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 73% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 55% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 55% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 53% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 47% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 50% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 52% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 52% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 54% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 52% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 54% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 51% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 52% Analysis Date = 12/07/14 SpikeMix = ERA 0318-14-02: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 83% Analysis Date = 11/04/14 SpikeMix = Abs 041814: 8 µl & ERA 0318-14-02: 8 µl Pct Recovery = 69% Analysis Date = 04/30/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 73% Analysis Date = 02/10/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 59% Analysis Date = 10/24/14 SpikeMix = ERA 0319-14-05: 8 µl & Abs 041614: 8 µl Pct Recovery = 75% Analysis Date = 10/10/14 SpikeMix = Abs 041814: 30 µl & ERA 0318-14-02: 30 µl Pct Recovery = 56% Analysis Date = 08/30/14 SpikeMix = ERA 0318-14-02: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 74% Analysis Date = 07/20/14 SpikeMix = ERA 0318-14-02: 30 µl & Abs 041714: 30 µl Pct Recovery = 57% Analysis Date = 09/12/14 SpikeMix = Abs 041614: 30 µl & ERA 0319-14-04: 30 µl Pct Recovery = 56% Analysis Date = 07/13/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 57% Analysis Date = 06/28/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 57% Analysis Date = 05/30/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 65% Analysis Date = 05/17/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 62% Analysis Date = 11/25/15 SpikeMix = Abs 050115: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 71% Analysis Date = 11/24/15 SpikeMix = ERA 0406-15-09: 20 µl & Abs 050115: 20 µl Pct Recovery = 74% Analysis Date = 08/27/15 SpikeMix = Abs 052215: 20 µl & Abs 050115: 20 µl Pct Recovery = 54% Analysis Date = 08/11/15 SpikeMix = Abs 050115: 20 µl & Abs 051315: 20 µl Pct Recovery = 44% Analysis Date = 07/09/15 SpikeMix = Abs 050115: 20 µl & Abs 052215: 20 µl Pct Recovery = 59% Analysis Date = 06/09/15 SpikeMix = Abs 051315: 20 µl & Abs 050115: 20 µl Pct Recovery = 59% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 54% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 48% Analysis Date = 04/27/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 84% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 62% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 73% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 45% Analysis Date = 11/24/15 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 76% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-09: 20 µl Pct Recovery = 60% Analysis Date = 09/15/15 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 56% Analysis Date = 01/04/17 Pct Recovery = 53% Analysis Date = 12/31/16 Pct Recovery = 53% Analysis Date = 12/31/16 Pct Recovery = 53% Analysis Date = 12/26/16 Pct Recovery = 54% Analysis Date = 12/26/16 Pct Recovery = 54% Analysis Date = 12/21/16 Pct Recovery = 54% Analysis Date = 12/21/16 Pct Recovery = 54% Analysis Date = 12/16/16 Pct Recovery = 54% Analysis Date = 12/16/16 Pct Recovery = 54% Analysis Date = 12/11/16 Pct Recovery = 54% Analysis Date = 12/11/16 Pct Recovery = 54% Analysis Date = 12/07/16 Pct Recovery = 54% Analysis Date = 12/07/16 Pct Recovery = 54% Analysis Date = 12/02/16 Pct Recovery = 54% Analysis Date = 12/02/16 Pct Recovery = 54% Analysis Date = 11/27/16 Pct Recovery = 54% Analysis Date = 11/27/16 Pct Recovery = 54% Analysis Date = 11/22/16 Pct Recovery = 54% Analysis Date = 11/22/16 Pct Recovery = 54% Analysis Date = 11/17/16 Pct Recovery = 55% Analysis Date = 11/17/16 Pct Recovery = 55% Analysis Date = 11/12/16 Pct Recovery = 55% Analysis Date = 11/12/16 Pct Recovery = 55% Analysis Date = 11/08/16 Pct Recovery = 55% Analysis Date = 11/08/16 Pct Recovery = 55% Analysis Date = 11/03/16 Pct Recovery = 55% Analysis Date = 11/03/16 Pct Recovery = 55% Analysis Date = 10/29/16 Pct Recovery = 55% Analysis Date = 10/29/16 Pct Recovery = 55% Analysis Date = 10/24/16 Pct Recovery = 55% Analysis Date = 10/24/16 Pct Recovery = 55% Analysis Date = 10/19/16 Pct Recovery = 55% Analysis Date = 10/19/16 Pct Recovery = 55% Analysis Date = 10/15/16 Pct Recovery = 55% Analysis Date = 10/15/16 Pct Recovery = 55% Analysis Date = 10/10/16 Pct Recovery = 56% Analysis Date = 10/10/16 Pct Recovery = 56% Analysis Date = 10/05/16 Pct Recovery = 56% Analysis Date = 10/05/16 Pct Recovery = 56% Analysis Date = 09/30/16 Pct Recovery = 56% Analysis Date = 09/30/16 Pct Recovery = 56% Analysis Date = 09/25/16 Pct Recovery = 56% Analysis Date = 09/25/16 Pct Recovery = 56% Analysis Date = 09/20/16 Pct Recovery = 56% Analysis Date = 09/20/16 Pct Recovery = 56% Analysis Date = 09/16/16 Pct Recovery = 56% Analysis Date = 09/16/16 Pct Recovery = 56% Analysis Date = 09/11/16 Pct Recovery = 56% Analysis Date = 09/11/16 Pct Recovery = 56% Analysis Date = 09/06/16 Pct Recovery = 56% Analysis Date = 09/06/16 Pct Recovery = 56% Analysis Date = 09/01/16 Pct Recovery = 57% Analysis Date = 09/01/16 Pct Recovery = 57% Analysis Date = 08/27/16 Pct Recovery = 57% Analysis Date = 08/27/16 Pct Recovery = 57% Analysis Date = 08/23/16 Pct Recovery = 57% Analysis Date = 08/23/16 Pct Recovery = 57% Analysis Date = 08/18/16 Pct Recovery = 57% Analysis Date = 08/18/16 Pct Recovery = 57% Analysis Date = 08/13/16 Pct Recovery = 57% Analysis Date = 08/13/16 Pct Recovery = 57% Analysis Date = 08/08/16 Pct Recovery = 57% Analysis Date = 08/08/16 Pct Recovery = 57% Analysis Date = 08/03/16 Pct Recovery = 57% Analysis Date = 08/03/16 Pct Recovery = 57% Analysis Date = 07/29/16 Pct Recovery = 58% Analysis Date = 07/29/16 Pct Recovery = 58% Analysis Date = 07/25/16 Pct Recovery = 58% Analysis Date = 07/25/16 Pct Recovery = 58% Analysis Date = 07/20/16 Pct Recovery = 58% Analysis Date = 07/20/16 Pct Recovery = 58% Analysis Date = 07/15/16 Pct Recovery = 58% Analysis Date = 07/15/16 Pct Recovery = 58% Analysis Date = 07/10/16 Pct Recovery = 58% Analysis Date = 07/10/16 Pct Recovery = 58% Analysis Date = 07/05/16 Pct Recovery = 58% Analysis Date = 07/05/16 Pct Recovery = 58% Analysis Date = 07/01/16 Pct Recovery = 59% Analysis Date = 07/01/16 Pct Recovery = 59% Analysis Date = 06/26/16 Pct Recovery = 59% Analysis Date = 06/26/16 Pct Recovery = 59% Analysis Date = 06/21/16 Pct Recovery = 59% Analysis Date = 06/21/16 Pct Recovery = 59% Analysis Date = 06/16/16 Pct Recovery = 59% Analysis Date = 06/16/16 Pct Recovery = 59% Analysis Date = 06/11/16 Pct Recovery = 59% Analysis Date = 06/11/16 Pct Recovery = 59% Analysis Date = 06/06/16 Pct Recovery = 59% Analysis Date = 06/06/16 Pct Recovery = 59% Analysis Date = 06/02/16 Pct Recovery = 60% Analysis Date = 06/02/16 Pct Recovery = 60% Analysis Date = 05/28/16 Pct Recovery = 60% Analysis Date = 05/28/16 Pct Recovery = 60% Analysis Date = 05/23/16 Pct Recovery = 60% Analysis Date = 05/23/16 Pct Recovery = 60% Analysis Date = 05/18/16 Pct Recovery = 60% Analysis Date = 05/18/16 Pct Recovery = 60% Analysis Date = 05/13/16 Pct Recovery = 60% Analysis Date = 05/13/16 Pct Recovery = 60% Analysis Date = 05/08/16 Pct Recovery = 60% Analysis Date = 05/08/16 Pct Recovery = 60% Analysis Date = 05/04/16 Pct Recovery = 60% Analysis Date = 05/04/16 Pct Recovery = 60% Analysis Date = 04/29/16 Pct Recovery = 61% Analysis Date = 04/29/16 Pct Recovery = 61% Analysis Date = 04/24/16 Pct Recovery = 61% Analysis Date = 04/24/16 Pct Recovery = 61% Analysis Date = 04/19/16 Pct Recovery = 61% Analysis Date = 04/19/16 Pct Recovery = 61% Analysis Date = 04/14/16 Pct Recovery = 61% Analysis Date = 04/14/16 Pct Recovery = 61% Analysis Date = 04/10/16 Pct Recovery = 61% Analysis Date = 04/10/16 Pct Recovery = 61% Analysis Date = 04/05/16 Pct Recovery = 61% Analysis Date = 04/05/16 Pct Recovery = 61% Analysis Date = 03/31/16 Pct Recovery = 61% Analysis Date = 03/31/16 Pct Recovery = 61% Analysis Date = 03/26/16 Pct Recovery = 61% Analysis Date = 03/26/16 Pct Recovery = 61% Analysis Date = 03/21/16 Pct Recovery = 62% Analysis Date = 03/21/16 Pct Recovery = 62% Analysis Date = 03/16/16 Pct Recovery = 62% Analysis Date = 03/16/16 Pct Recovery = 62% Analysis Date = 03/12/16 Pct Recovery = 62% Analysis Date = 03/12/16 Pct Recovery = 62% Analysis Date = 03/07/16 Pct Recovery = 62% Analysis Date = 03/07/16 Pct Recovery = 62% Analysis Date = 03/02/16 Pct Recovery = 62% Analysis Date = 03/02/16 Pct Recovery = 62% Analysis Date = 02/26/16 Pct Recovery = 62% Analysis Date = 02/26/16 Pct Recovery = 62% Analysis Date = 02/21/16 Pct Recovery = 62% Analysis Date = 02/21/16 Pct Recovery = 62% Analysis Date = 02/17/16 Pct Recovery = 62% Analysis Date = 02/17/16 Pct Recovery = 62% Analysis Date = 02/12/16 Pct Recovery = 62% Analysis Date = 02/12/16 Pct Recovery = 62% Analysis Date = 02/07/16 Pct Recovery = 62% Analysis Date = 02/07/16 Pct Recovery = 62% Analysis Date = 02/02/16 Pct Recovery = 62% Analysis Date = 02/02/16 Pct Recovery = 62% Analysis Date = 01/28/16 Pct Recovery = 63% Analysis Date = 01/28/16 Pct Recovery = 63% Analysis Date = 01/23/16 Pct Recovery = 63% Analysis Date = 01/23/16 Pct Recovery = 63% Analysis Date = 01/19/16 Pct Recovery = 63% Analysis Date = 01/19/16 Pct Recovery = 63% Analysis Date = 01/14/16 Pct Recovery = 63% Analysis Date = 01/14/16 Pct Recovery = 63% Analysis Date = 01/09/16 Pct Recovery = 63% Analysis Date = 01/09/16 Pct Recovery = 63% Analysis Date = 01/04/16 Pct Recovery = 63% Analysis Date = 01/04/16 Pct Recovery = 63% Analysis Date = 12/30/15 Pct Recovery = 63% Analysis Date = 12/30/15 Pct Recovery = 63% Analysis Date = 12/26/15 Pct Recovery = 63% Analysis Date = 12/26/15 Pct Recovery = 63% Analysis Date = 12/21/15 Pct Recovery = 63% Analysis Date = 12/21/15 Pct Recovery = 63% Analysis Date = 12/16/15 Pct Recovery = 63% Analysis Date = 12/16/15 Pct Recovery = 63% Analysis Date = 12/11/15 Pct Recovery = 63% Analysis Date = 12/11/15 Pct Recovery = 63% Analysis Date = 12/06/15 Pct Recovery = 63% Analysis Date = 12/06/15 Pct Recovery = 63% Analysis Date = 12/01/15 Pct Recovery = 63% Analysis Date = 12/01/15 Pct Recovery = 63% Analysis Date = 11/27/15 Pct Recovery = 63% Analysis Date = 11/27/15 Pct Recovery = 63% Analysis Date = 11/22/15 Pct Recovery = 63% Analysis Date = 11/22/15 Pct Recovery = 63% Analysis Date = 11/17/15 Pct Recovery = 63% Analysis Date = 11/17/15 Pct Recovery = 63% Analysis Date = 11/12/15 Pct Recovery = 64% Analysis Date = 11/12/15 Pct Recovery = 64% Analysis Date = 11/07/15 Pct Recovery = 64% Analysis Date = 11/07/15 Pct Recovery = 64% Analysis Date = 11/03/15 Pct Recovery = 64% Analysis Date = 11/03/15 Pct Recovery = 64% Analysis Date = 10/29/15 Pct Recovery = 64% Analysis Date = 10/29/15 Pct Recovery = 64% Analysis Date = 10/24/15 Pct Recovery = 64% Analysis Date = 10/24/15 Pct Recovery = 64% Analysis Date = 10/19/15 Pct Recovery = 64% Analysis Date = 10/19/15 Pct Recovery = 64% Analysis Date = 10/14/15 Pct Recovery = 64% Analysis Date = 10/14/15 Pct Recovery = 64% Analysis Date = 10/09/15 Pct Recovery = 64% Analysis Date = 10/09/15 Pct Recovery = 64% Analysis Date = 10/05/15 Pct Recovery = 64% Analysis Date = 10/05/15 Pct Recovery = 64% Analysis Date = 09/30/15 Pct Recovery = 65% Analysis Date = 09/30/15 Pct Recovery = 65% Analysis Date = 09/25/15 Pct Recovery = 65% Analysis Date = 09/25/15 Pct Recovery = 65% Analysis Date = 09/20/15 Pct Recovery = 65% Analysis Date = 09/20/15 Pct Recovery = 65% Analysis Date = 09/15/15 Pct Recovery = 65% Analysis Date = 09/15/15 Pct Recovery = 65% Analysis Date = 09/10/15 Pct Recovery = 65% Analysis Date = 09/10/15 Pct Recovery = 65% Analysis Date = 09/06/15 Pct Recovery = 65% Analysis Date = 09/06/15 Pct Recovery = 65% Analysis Date = 09/01/15 Pct Recovery = 65% Analysis Date = 09/01/15 Pct Recovery = 65% Analysis Date = 08/27/15 Pct Recovery = 65% Analysis Date = 08/27/15 Pct Recovery = 65% Analysis Date = 08/22/15 Pct Recovery = 65% Analysis Date = 08/22/15 Pct Recovery = 65% Analysis Date = 08/17/15 Pct Recovery = 66% Analysis Date = 08/17/15 Pct Recovery = 66% Analysis Date = 08/13/15 Pct Recovery = 66% Analysis Date = 08/13/15 Pct Recovery = 66% Analysis Date = 08/08/15 Pct Recovery = 66% Analysis Date = 08/08/15 Pct Recovery = 66% Analysis Date = 08/03/15 Pct Recovery = 66% Analysis Date = 08/03/15 Pct Recovery = 66% Analysis Date = 07/29/15 Pct Recovery = 66% Analysis Date = 07/29/15 Pct Recovery = 66% Analysis Date = 07/24/15 Pct Recovery = 66% Analysis Date = 07/24/15 Pct Recovery = 66% Analysis Date = 07/19/15 Pct Recovery = 66% Analysis Date = 07/19/15 Pct Recovery = 66% Analysis Date = 07/15/15 Pct Recovery = 66% Analysis Date = 07/15/15 Pct Recovery = 66% Analysis Date = 07/10/15 Pct Recovery = 66% Analysis Date = 07/10/15 Pct Recovery = 66% Analysis Date = 07/05/15 Pct Recovery = 66% Analysis Date = 07/05/15 Pct Recovery = 66% Analysis Date = 06/30/15 Pct Recovery = 66% Analysis Date = 06/30/15 Pct Recovery = 66% Analysis Date = 06/25/15 Pct Recovery = 66% Analysis Date = 06/25/15 Pct Recovery = 66% Analysis Date = 06/21/15 Pct Recovery = 66% Analysis Date = 06/21/15 Pct Recovery = 66% Analysis Date = 06/16/15 Pct Recovery = 66% Analysis Date = 06/16/15 Pct Recovery = 66% Analysis Date = 06/11/15 Pct Recovery = 66% Analysis Date = 06/11/15 Pct Recovery = 66% Analysis Date = 06/06/15 Pct Recovery = 66% Analysis Date = 06/06/15 Pct Recovery = 66% Analysis Date = 06/01/15 Pct Recovery = 66% Analysis Date = 06/01/15 Pct Recovery = 66% Analysis Date = 05/27/15 Pct Recovery = 66% Analysis Date = 05/27/15 Pct Recovery = 66% Analysis Date = 05/23/15 Pct Recovery = 66% Analysis Date = 05/23/15 Pct Recovery = 66% Analysis Date = 05/18/15 Pct Recovery = 66% Analysis Date = 05/18/15 Pct Recovery = 66% Analysis Date = 05/13/15 Pct Recovery = 66% Analysis Date = 05/13/15 Pct Recovery = 66% Analysis Date = 05/08/15 Pct Recovery = 66% Analysis Date = 05/08/15 Pct Recovery = 66% Analysis Date = 05/03/15 Pct Recovery = 67% Analysis Date = 05/03/15 Pct Recovery = 67% Analysis Date = 04/29/15 Pct Recovery = 67% Analysis Date = 04/29/15 Pct Recovery = 67% Analysis Date = 04/24/15 Pct Recovery = 67% Analysis Date = 04/24/15 Pct Recovery = 67% Analysis Date = 04/19/15 Pct Recovery = 67% Analysis Date = 04/19/15 Pct Recovery = 67% Analysis Date = 04/14/15 Pct Recovery = 67% Analysis Date = 04/14/15 Pct Recovery = 67% Analysis Date = 04/09/15 Pct Recovery = 67% Analysis Date = 04/09/15 Pct Recovery = 67% Analysis Date = 04/04/15 Pct Recovery = 67% Analysis Date = 04/04/15 Pct Recovery = 67% Analysis Date = 03/31/15 Pct Recovery = 67% Analysis Date = 03/31/15 Pct Recovery = 67% Analysis Date = 03/26/15 Pct Recovery = 67% Analysis Date = 03/26/15 Pct Recovery = 67% Analysis Date = 03/21/15 Pct Recovery = 67% Analysis Date = 03/21/15 Pct Recovery = 67% Analysis Date = 03/16/15 Pct Recovery = 67% Analysis Date = 03/16/15 Pct Recovery = 67% Analysis Date = 03/11/15 Pct Recovery = 67% Analysis Date = 03/11/15 Pct Recovery = 67% Analysis Date = 03/07/15 Pct Recovery = 67% Analysis Date = 03/07/15 Pct Recovery = 67% Analysis Date = 03/02/15 Pct Recovery = 67% Analysis Date = 03/02/15 Pct Recovery = 67% Analysis Date = 02/25/15 Pct Recovery = 67% Analysis Date = 02/25/15 Pct Recovery = 67% Analysis Date = 02/20/15 Pct Recovery = 67% Analysis Date = 02/20/15 Pct Recovery = 67% Analysis Date = 02/15/15 Pct Recovery = 67% Analysis Date = 02/15/15 Pct Recovery = 67% Analysis Date = 02/10/15 Pct Recovery = 67% Analysis Date = 02/10/15 Pct Recovery = 67% Analysis Date = 02/06/15 Pct Recovery = 67% Analysis Date = 02/06/15 Pct Recovery = 67% Analysis Date = 02/01/15 Pct Recovery = 67% Analysis Date = 02/01/15 Pct Recovery = 67% Analysis Date = 01/27/15 Pct Recovery = 67% Analysis Date = 01/27/15 Pct Recovery = 67% Analysis Date = 01/22/15 Pct Recovery = 67% Analysis Date = 01/22/15 Pct Recovery = 67% Analysis Date = 01/17/15 Pct Recovery = 67% Analysis Date = 01/17/15 Pct Recovery = 67% Analysis Date = 01/12/15 Pct Recovery = 67% Analysis Date = 01/12/15 Pct Recovery = 67% Analysis Date = 01/08/15 Pct Recovery = 67% Analysis Date = 01/08/15 Pct Recovery = 67% Analysis Date = 01/03/15 Pct Recovery = 67% Analysis Date = 01/03/15 Pct Recovery = 67% Analysis Date = 12/29/14 Pct Recovery = 67% Analysis Date = 12/29/14 Pct Recovery = 67% Analysis Date = 12/24/14 Pct Recovery = 67% Analysis Date = 12/24/14 Pct Recovery = 67% Analysis Date = 12/19/14 Pct Recovery = 67% Analysis Date = 12/19/14 Pct Recovery = 67% Analysis Date = 12/15/14 Pct Recovery = 67% Analysis Date = 12/15/14 Pct Recovery = 67% Analysis Date = 12/10/14 Pct Recovery = 67% Analysis Date = 12/10/14 Pct Recovery = 67% Analysis Date = 12/05/14 Pct Recovery = 67% Analysis Date = 12/05/14 Pct Recovery = 67% Analysis Date = 11/30/14 Pct Recovery = 67% Analysis Date = 11/30/14 Pct Recovery = 67% Analysis Date = 11/25/14 Pct Recovery = 67% Analysis Date = 11/25/14 Pct Recovery = 67% Analysis Date = 11/20/14 Pct Recovery = 67% Analysis Date = 11/20/14 Pct Recovery = 67% Analysis Date = 11/16/14 Pct Recovery = 67% Analysis Date = 11/16/14 Pct Recovery = 67% Analysis Date = 11/11/14 Pct Recovery = 67% Analysis Date = 11/11/14 Pct Recovery = 67% Analysis Date = 11/06/14 Pct Recovery = 67% Analysis Date = 11/06/14 Pct Recovery = 67% Analysis Date = 11/01/14 Pct Recovery = 67% Analysis Date = 11/01/14 Pct Recovery = 67% Analysis Date = 10/27/14 Pct Recovery = 67% Analysis Date = 10/27/14 Pct Recovery = 67% Analysis Date = 10/23/14 Pct Recovery = 67% Analysis Date = 10/23/14 Pct Recovery = 67% Analysis Date = 10/18/14 Pct Recovery = 67% Analysis Date = 10/18/14 Pct Recovery = 67% Analysis Date = 10/13/14 Pct Recovery = 67% Analysis Date = 10/13/14 Pct Recovery = 67% Analysis Date = 10/08/14 Pct Recovery = 67% Analysis Date = 10/08/14 Pct Recovery = 67% Analysis Date = 10/03/14 Pct Recovery = 67% Analysis Date = 10/03/14 Pct Recovery = 67% Analysis Date = 09/28/14 Pct Recovery = 67% Analysis Date = 09/28/14 Pct Recovery = 67% Analysis Date = 09/24/14 Pct Recovery = 67% Analysis Date = 09/24/14 Pct Recovery = 67% Analysis Date = 09/19/14 Pct Recovery = 67% Analysis Date = 09/19/14 Pct Recovery = 67% Analysis Date = 09/14/14 Pct Recovery = 67% Analysis Date = 09/14/14 Pct Recovery = 67% Analysis Date = 09/09/14 Pct Recovery = 67% Analysis Date = 09/09/14 Pct Recovery = 67% Analysis Date = 09/04/14 Pct Recovery = 67% Analysis Date = 09/04/14 Pct Recovery = 67% Analysis Date = 08/31/14 Pct Recovery = 67% Analysis Date = 08/31/14 Pct Recovery = 67% Analysis Date = 08/26/14 Pct Recovery = 67% Analysis Date = 08/26/14 Pct Recovery = 67% Analysis Date = 08/21/14 Pct Recovery = 67% Analysis Date = 08/21/14 Pct Recovery = 67% Analysis Date = 08/16/14 Pct Recovery = 67% Analysis Date = 08/16/14 Pct Recovery = 67% Analysis Date = 08/11/14 Pct Recovery = 67% Analysis Date = 08/11/14 Pct Recovery = 67% Analysis Date = 08/06/14 Pct Recovery = 67% Analysis Date = 08/06/14 Pct Recovery = 67% Analysis Date = 08/02/14 Pct Recovery = 67% Analysis Date = 08/02/14 Pct Recovery = 67% Analysis Date = 07/28/14 Pct Recovery = 67% Analysis Date = 07/28/14 Pct Recovery = 67% Analysis Date = 07/23/14 Pct Recovery = 67% Analysis Date = 07/23/14 Pct Recovery = 67% Analysis Date = 07/18/14 Pct Recovery = 67% Analysis Date = 07/18/14 Pct Recovery = 67% Analysis Date = 07/13/14 Pct Recovery = 66% Analysis Date = 07/13/14 Pct Recovery = 66% Analysis Date = 07/09/14 Pct Recovery = 66% Analysis Date = 07/09/14 Pct Recovery = 66% Analysis Date = 07/04/14 Pct Recovery = 66% Analysis Date = 07/04/14 Pct Recovery = 66% Analysis Date = 06/29/14 Pct Recovery = 66% Analysis Date = 06/29/14 Pct Recovery = 66% Analysis Date = 06/24/14 Pct Recovery = 66% Analysis Date = 06/24/14 Pct Recovery = 66% Analysis Date = 06/19/14 Pct Recovery = 66% Analysis Date = 06/19/14 Pct Recovery = 66% Analysis Date = 06/14/14 Pct Recovery = 66% Analysis Date = 06/14/14 Pct Recovery = 66% Analysis Date = 06/10/14 Pct Recovery = 66% Analysis Date = 06/10/14 Pct Recovery = 66% Analysis Date = 06/05/14 Pct Recovery = 66% Analysis Date = 06/05/14 Pct Recovery = 66% Analysis Date = 05/31/14 Pct Recovery = 66% Analysis Date = 05/31/14 Pct Recovery = 66% Analysis Date = 05/26/14 Pct Recovery = 66% Analysis Date = 05/26/14 Pct Recovery = 66% Analysis Date = 05/21/14 Pct Recovery = 66% Analysis Date = 05/21/14 Pct Recovery = 66% Analysis Date = 05/17/14 Pct Recovery = 66% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
FADROZOLE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 76 62% 11% 60% 11%
Total 76 62% 11% 60% 11%

Sample Statistics
FADROZOLE

Characteristic N % % Basis
Plotted 76 99% Spiked
Estimated Values 5 6% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 77 .  
False Negatives 1 1% 1 out of 77
Not Spiked 38 .  
False Positives 2 5% 2 out of 38

BQS OBSP Determination:
FAMOTIDINE
METHOD: 2440 , TESTIDCODE: 68000LCM56
Open Data Set

Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 232% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-04: 15 µl & Abs 041814: 15 µl Pct Recovery = 263% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 23% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 19% Analysis Date = 11/24/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 69% Analysis Date = 11/05/15 SpikeMix = ERA 0406-15-08: 80 µl & Abs 052215: 80 µl Pct Recovery = 5% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 39% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 39% Analysis Date = 09/24/16 SpikeMix = Crescent EN160610015: 80 µl & Abs 061416: 80 µl Pct Recovery = 45% Analysis Date = 09/24/16 SpikeMix = Abs 061416: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 45% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 6% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 5% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 12% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 15% Analysis Date = 05/07/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 50% Analysis Date = 04/29/15 SpikeMix = ERA 0319-14-05: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 45% Analysis Date = 01/16/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 66% Analysis Date = 12/07/14 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 55% Analysis Date = 12/06/14 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 53% Analysis Date = 08/28/14 SpikeMix = ERA 0319-14-04: 60 µl & ERA 0319-14-05: 60 µl Pct Recovery = 72% Analysis Date = 07/26/14 SpikeMix = ERA 0319-14-05: 60 µl & ERA 0318-14-02: 60 µl Pct Recovery = 86% Analysis Date = 07/12/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 53% Analysis Date = 06/22/14 SpikeMix = Abs 041814: 60 µl & Abs 041614: 60 µl Pct Recovery = 150% Analysis Date = 11/04/15 SpikeMix = ERA 0406-15-07A: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 7% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 17% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 15% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 10% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 8% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 17% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 19% Analysis Date = 11/04/14 SpikeMix = Abs 041714: 8 µl & ERA 0319-14-05: 8 µl Pct Recovery = 44% Analysis Date = 10/24/14 SpikeMix = ERA 0319-14-05: 8 µl & Abs 041614: 8 µl Pct Recovery = 61% Analysis Date = 04/10/15 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 126% Analysis Date = 11/04/14 SpikeMix = Abs 041814: 8 µl & ERA 0318-14-02: 8 µl Pct Recovery = 92% Analysis Date = 08/30/14 SpikeMix = ERA 0318-14-02: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 59% Analysis Date = 08/16/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 64% Analysis Date = 07/13/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 64% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-08: 20 µl & ERA 0406-15-09: 20 µl Pct Recovery = 28% Analysis Date = 06/26/15 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 54% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 59% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 65% Analysis Date = 12/16/16 Pct Recovery = 32% Analysis Date = 12/11/16 Pct Recovery = 31% Analysis Date = 12/11/16 Pct Recovery = 31% Analysis Date = 12/06/16 Pct Recovery = 31% Analysis Date = 12/06/16 Pct Recovery = 31% Analysis Date = 12/02/16 Pct Recovery = 31% Analysis Date = 12/02/16 Pct Recovery = 31% Analysis Date = 11/27/16 Pct Recovery = 30% Analysis Date = 11/27/16 Pct Recovery = 30% Analysis Date = 11/23/16 Pct Recovery = 30% Analysis Date = 11/23/16 Pct Recovery = 30% Analysis Date = 11/18/16 Pct Recovery = 30% Analysis Date = 11/18/16 Pct Recovery = 30% Analysis Date = 11/14/16 Pct Recovery = 30% Analysis Date = 11/14/16 Pct Recovery = 30% Analysis Date = 11/09/16 Pct Recovery = 29% Analysis Date = 11/09/16 Pct Recovery = 29% Analysis Date = 11/05/16 Pct Recovery = 29% Analysis Date = 11/05/16 Pct Recovery = 29% Analysis Date = 10/31/16 Pct Recovery = 29% Analysis Date = 10/31/16 Pct Recovery = 29% Analysis Date = 10/27/16 Pct Recovery = 29% Analysis Date = 10/27/16 Pct Recovery = 29% Analysis Date = 10/22/16 Pct Recovery = 28% Analysis Date = 10/22/16 Pct Recovery = 28% Analysis Date = 10/17/16 Pct Recovery = 28% Analysis Date = 10/17/16 Pct Recovery = 28% Analysis Date = 10/13/16 Pct Recovery = 28% Analysis Date = 10/13/16 Pct Recovery = 28% Analysis Date = 10/08/16 Pct Recovery = 28% Analysis Date = 10/08/16 Pct Recovery = 28% Analysis Date = 10/04/16 Pct Recovery = 27% Analysis Date = 10/04/16 Pct Recovery = 27% Analysis Date = 09/29/16 Pct Recovery = 27% Analysis Date = 09/29/16 Pct Recovery = 27% Analysis Date = 09/25/16 Pct Recovery = 27% Analysis Date = 09/25/16 Pct Recovery = 27% Analysis Date = 09/20/16 Pct Recovery = 27% Analysis Date = 09/20/16 Pct Recovery = 27% Analysis Date = 09/16/16 Pct Recovery = 27% Analysis Date = 09/16/16 Pct Recovery = 27% Analysis Date = 09/11/16 Pct Recovery = 26% Analysis Date = 09/11/16 Pct Recovery = 26% Analysis Date = 09/07/16 Pct Recovery = 26% Analysis Date = 09/07/16 Pct Recovery = 26% Analysis Date = 09/02/16 Pct Recovery = 26% Analysis Date = 09/02/16 Pct Recovery = 26% Analysis Date = 08/29/16 Pct Recovery = 26% Analysis Date = 08/29/16 Pct Recovery = 26% Analysis Date = 08/24/16 Pct Recovery = 26% Analysis Date = 08/24/16 Pct Recovery = 26% Analysis Date = 08/19/16 Pct Recovery = 26% Analysis Date = 08/19/16 Pct Recovery = 26% Analysis Date = 08/15/16 Pct Recovery = 25% Analysis Date = 08/15/16 Pct Recovery = 25% Analysis Date = 08/10/16 Pct Recovery = 25% Analysis Date = 08/10/16 Pct Recovery = 25% Analysis Date = 08/06/16 Pct Recovery = 25% Analysis Date = 08/06/16 Pct Recovery = 25% Analysis Date = 08/01/16 Pct Recovery = 25% Analysis Date = 08/01/16 Pct Recovery = 25% Analysis Date = 07/28/16 Pct Recovery = 25% Analysis Date = 07/28/16 Pct Recovery = 25% Analysis Date = 07/23/16 Pct Recovery = 25% Analysis Date = 07/23/16 Pct Recovery = 25% Analysis Date = 07/19/16 Pct Recovery = 25% Analysis Date = 07/19/16 Pct Recovery = 25% Analysis Date = 07/14/16 Pct Recovery = 25% Analysis Date = 07/14/16 Pct Recovery = 25% Analysis Date = 07/10/16 Pct Recovery = 25% Analysis Date = 07/10/16 Pct Recovery = 25% Analysis Date = 07/05/16 Pct Recovery = 25% Analysis Date = 07/05/16 Pct Recovery = 25% Analysis Date = 07/01/16 Pct Recovery = 26% Analysis Date = 07/01/16 Pct Recovery = 26% Analysis Date = 06/26/16 Pct Recovery = 26% Analysis Date = 06/26/16 Pct Recovery = 26% Analysis Date = 06/21/16 Pct Recovery = 26% Analysis Date = 06/21/16 Pct Recovery = 26% Analysis Date = 06/17/16 Pct Recovery = 26% Analysis Date = 06/17/16 Pct Recovery = 26% Analysis Date = 06/12/16 Pct Recovery = 27% Analysis Date = 06/12/16 Pct Recovery = 27% Analysis Date = 06/08/16 Pct Recovery = 27% Analysis Date = 06/08/16 Pct Recovery = 27% Analysis Date = 06/03/16 Pct Recovery = 27% Analysis Date = 06/03/16 Pct Recovery = 27% Analysis Date = 05/30/16 Pct Recovery = 28% Analysis Date = 05/30/16 Pct Recovery = 28% Analysis Date = 05/25/16 Pct Recovery = 28% Analysis Date = 05/25/16 Pct Recovery = 28% Analysis Date = 05/21/16 Pct Recovery = 28% Analysis Date = 05/21/16 Pct Recovery = 28% Analysis Date = 05/16/16 Pct Recovery = 28% Analysis Date = 05/16/16 Pct Recovery = 28% Analysis Date = 05/12/16 Pct Recovery = 29% Analysis Date = 05/12/16 Pct Recovery = 29% Analysis Date = 05/07/16 Pct Recovery = 29% Analysis Date = 05/07/16 Pct Recovery = 29% Analysis Date = 05/03/16 Pct Recovery = 29% Analysis Date = 05/03/16 Pct Recovery = 29% Analysis Date = 04/28/16 Pct Recovery = 29% Analysis Date = 04/28/16 Pct Recovery = 29% Analysis Date = 04/23/16 Pct Recovery = 30% Analysis Date = 04/23/16 Pct Recovery = 30% Analysis Date = 04/19/16 Pct Recovery = 30% Analysis Date = 04/19/16 Pct Recovery = 30% Analysis Date = 04/14/16 Pct Recovery = 30% Analysis Date = 04/14/16 Pct Recovery = 30% Analysis Date = 04/10/16 Pct Recovery = 30% Analysis Date = 04/10/16 Pct Recovery = 30% Analysis Date = 04/05/16 Pct Recovery = 31% Analysis Date = 04/05/16 Pct Recovery = 31% Analysis Date = 04/01/16 Pct Recovery = 31% Analysis Date = 04/01/16 Pct Recovery = 31% Analysis Date = 03/27/16 Pct Recovery = 31% Analysis Date = 03/27/16 Pct Recovery = 31% Analysis Date = 03/23/16 Pct Recovery = 31% Analysis Date = 03/23/16 Pct Recovery = 31% Analysis Date = 03/18/16 Pct Recovery = 32% Analysis Date = 03/18/16 Pct Recovery = 32% Analysis Date = 03/14/16 Pct Recovery = 32% Analysis Date = 03/14/16 Pct Recovery = 32% Analysis Date = 03/09/16 Pct Recovery = 32% Analysis Date = 03/09/16 Pct Recovery = 32% Analysis Date = 03/04/16 Pct Recovery = 33% Analysis Date = 03/04/16 Pct Recovery = 33% Analysis Date = 02/29/16 Pct Recovery = 33% Analysis Date = 02/29/16 Pct Recovery = 33% Analysis Date = 02/24/16 Pct Recovery = 33% Analysis Date = 02/24/16 Pct Recovery = 33% Analysis Date = 02/20/16 Pct Recovery = 33% Analysis Date = 02/20/16 Pct Recovery = 33% Analysis Date = 02/15/16 Pct Recovery = 34% Analysis Date = 02/15/16 Pct Recovery = 34% Analysis Date = 02/11/16 Pct Recovery = 34% Analysis Date = 02/11/16 Pct Recovery = 34% Analysis Date = 02/06/16 Pct Recovery = 34% Analysis Date = 02/06/16 Pct Recovery = 34% Analysis Date = 02/02/16 Pct Recovery = 34% Analysis Date = 02/02/16 Pct Recovery = 34% Analysis Date = 01/28/16 Pct Recovery = 35% Analysis Date = 01/28/16 Pct Recovery = 35% Analysis Date = 01/24/16 Pct Recovery = 35% Analysis Date = 01/24/16 Pct Recovery = 35% Analysis Date = 01/19/16 Pct Recovery = 35% Analysis Date = 01/19/16 Pct Recovery = 35% Analysis Date = 01/15/16 Pct Recovery = 35% Analysis Date = 01/15/16 Pct Recovery = 35% Analysis Date = 01/10/16 Pct Recovery = 36% Analysis Date = 01/10/16 Pct Recovery = 36% Analysis Date = 01/05/16 Pct Recovery = 36% Analysis Date = 01/05/16 Pct Recovery = 36% Analysis Date = 01/01/16 Pct Recovery = 36% Analysis Date = 01/01/16 Pct Recovery = 36% Analysis Date = 12/27/15 Pct Recovery = 36% Analysis Date = 12/27/15 Pct Recovery = 36% Analysis Date = 12/23/15 Pct Recovery = 37% Analysis Date = 12/23/15 Pct Recovery = 37% Analysis Date = 12/18/15 Pct Recovery = 37% Analysis Date = 12/18/15 Pct Recovery = 37% Analysis Date = 12/14/15 Pct Recovery = 37% Analysis Date = 12/14/15 Pct Recovery = 37% Analysis Date = 12/09/15 Pct Recovery = 38% Analysis Date = 12/09/15 Pct Recovery = 38% Analysis Date = 12/05/15 Pct Recovery = 38% Analysis Date = 12/05/15 Pct Recovery = 38% Analysis Date = 11/30/15 Pct Recovery = 38% Analysis Date = 11/30/15 Pct Recovery = 38% Analysis Date = 11/26/15 Pct Recovery = 38% Analysis Date = 11/26/15 Pct Recovery = 38% Analysis Date = 11/21/15 Pct Recovery = 39% Analysis Date = 11/21/15 Pct Recovery = 39% Analysis Date = 11/17/15 Pct Recovery = 39% Analysis Date = 11/17/15 Pct Recovery = 39% Analysis Date = 11/12/15 Pct Recovery = 39% Analysis Date = 11/12/15 Pct Recovery = 39% Analysis Date = 11/07/15 Pct Recovery = 39% Analysis Date = 11/07/15 Pct Recovery = 39% Analysis Date = 11/03/15 Pct Recovery = 40% Analysis Date = 11/03/15 Pct Recovery = 40% Analysis Date = 10/29/15 Pct Recovery = 41% Analysis Date = 10/29/15 Pct Recovery = 41% Analysis Date = 10/25/15 Pct Recovery = 42% Analysis Date = 10/25/15 Pct Recovery = 42% Analysis Date = 10/20/15 Pct Recovery = 43% Analysis Date = 10/20/15 Pct Recovery = 43% Analysis Date = 10/16/15 Pct Recovery = 44% Analysis Date = 10/16/15 Pct Recovery = 44% Analysis Date = 10/11/15 Pct Recovery = 45% Analysis Date = 10/11/15 Pct Recovery = 45% Analysis Date = 10/07/15 Pct Recovery = 47% Analysis Date = 10/07/15 Pct Recovery = 47% Analysis Date = 10/02/15 Pct Recovery = 48% Analysis Date = 10/02/15 Pct Recovery = 48% Analysis Date = 09/28/15 Pct Recovery = 49% Analysis Date = 09/28/15 Pct Recovery = 49% Analysis Date = 09/23/15 Pct Recovery = 50% Analysis Date = 09/23/15 Pct Recovery = 50% Analysis Date = 09/19/15 Pct Recovery = 51% Analysis Date = 09/19/15 Pct Recovery = 51% Analysis Date = 09/14/15 Pct Recovery = 52% Analysis Date = 09/14/15 Pct Recovery = 52% Analysis Date = 09/09/15 Pct Recovery = 53% Analysis Date = 09/09/15 Pct Recovery = 53% Analysis Date = 09/05/15 Pct Recovery = 54% Analysis Date = 09/05/15 Pct Recovery = 54% Analysis Date = 08/31/15 Pct Recovery = 55% Analysis Date = 08/31/15 Pct Recovery = 55% Analysis Date = 08/27/15 Pct Recovery = 56% Analysis Date = 08/27/15 Pct Recovery = 56% Analysis Date = 08/22/15 Pct Recovery = 58% Analysis Date = 08/22/15 Pct Recovery = 58% Analysis Date = 08/18/15 Pct Recovery = 59% Analysis Date = 08/18/15 Pct Recovery = 59% Analysis Date = 08/13/15 Pct Recovery = 60% Analysis Date = 08/13/15 Pct Recovery = 60% Analysis Date = 08/09/15 Pct Recovery = 61% Analysis Date = 08/09/15 Pct Recovery = 61% Analysis Date = 08/04/15 Pct Recovery = 62% Analysis Date = 08/04/15 Pct Recovery = 62% Analysis Date = 07/31/15 Pct Recovery = 63% Analysis Date = 07/31/15 Pct Recovery = 63% Analysis Date = 07/26/15 Pct Recovery = 64% Analysis Date = 07/26/15 Pct Recovery = 64% Analysis Date = 07/21/15 Pct Recovery = 65% Analysis Date = 07/21/15 Pct Recovery = 65% Analysis Date = 07/17/15 Pct Recovery = 66% Analysis Date = 07/17/15 Pct Recovery = 66% Analysis Date = 07/12/15 Pct Recovery = 67% Analysis Date = 07/12/15 Pct Recovery = 67% Analysis Date = 07/08/15 Pct Recovery = 69% Analysis Date = 07/08/15 Pct Recovery = 69% Analysis Date = 07/03/15 Pct Recovery = 70% Analysis Date = 07/03/15 Pct Recovery = 70% Analysis Date = 06/29/15 Pct Recovery = 71% Analysis Date = 06/29/15 Pct Recovery = 71% Analysis Date = 06/24/15 Pct Recovery = 72% Analysis Date = 06/24/15 Pct Recovery = 72% Analysis Date = 06/20/15 Pct Recovery = 72% Analysis Date = 06/20/15 Pct Recovery = 72% Analysis Date = 06/15/15 Pct Recovery = 72% Analysis Date = 06/15/15 Pct Recovery = 72% Analysis Date = 06/11/15 Pct Recovery = 73% Analysis Date = 06/11/15 Pct Recovery = 73% Analysis Date = 06/06/15 Pct Recovery = 73% Analysis Date = 06/06/15 Pct Recovery = 73% Analysis Date = 06/02/15 Pct Recovery = 73% Analysis Date = 06/02/15 Pct Recovery = 73% Analysis Date = 05/28/15 Pct Recovery = 74% Analysis Date = 05/28/15 Pct Recovery = 74% Analysis Date = 05/23/15 Pct Recovery = 74% Analysis Date = 05/23/15 Pct Recovery = 74% Analysis Date = 05/19/15 Pct Recovery = 74% Analysis Date = 05/19/15 Pct Recovery = 74% Analysis Date = 05/14/15 Pct Recovery = 75% Analysis Date = 05/14/15 Pct Recovery = 75% Analysis Date = 05/10/15 Pct Recovery = 75% Analysis Date = 05/10/15 Pct Recovery = 75% Analysis Date = 05/05/15 Pct Recovery = 75% Analysis Date = 05/05/15 Pct Recovery = 75% Analysis Date = 05/01/15 Pct Recovery = 76% Analysis Date = 05/01/15 Pct Recovery = 76% Analysis Date = 04/26/15 Pct Recovery = 76% Analysis Date = 04/26/15 Pct Recovery = 76% Analysis Date = 04/22/15 Pct Recovery = 76% Analysis Date = 04/22/15 Pct Recovery = 76% Analysis Date = 04/17/15 Pct Recovery = 77% Analysis Date = 04/17/15 Pct Recovery = 77% Analysis Date = 04/13/15 Pct Recovery = 77% Analysis Date = 04/13/15 Pct Recovery = 77% Analysis Date = 04/08/15 Pct Recovery = 77% Analysis Date = 04/08/15 Pct Recovery = 77% Analysis Date = 04/04/15 Pct Recovery = 77% Analysis Date = 04/04/15 Pct Recovery = 77% Analysis Date = 03/30/15 Pct Recovery = 78% Analysis Date = 03/30/15 Pct Recovery = 78% Analysis Date = 03/25/15 Pct Recovery = 78% Analysis Date = 03/25/15 Pct Recovery = 78% Analysis Date = 03/21/15 Pct Recovery = 78% Analysis Date = 03/21/15 Pct Recovery = 78% Analysis Date = 03/16/15 Pct Recovery = 79% Analysis Date = 03/16/15 Pct Recovery = 79% Analysis Date = 03/12/15 Pct Recovery = 79% Analysis Date = 03/12/15 Pct Recovery = 79% Analysis Date = 03/07/15 Pct Recovery = 79% Analysis Date = 03/07/15 Pct Recovery = 79% Analysis Date = 03/03/15 Pct Recovery = 79% Analysis Date = 03/03/15 Pct Recovery = 79% Analysis Date = 02/26/15 Pct Recovery = 80% Analysis Date = 02/26/15 Pct Recovery = 80% Analysis Date = 02/22/15 Pct Recovery = 80% Analysis Date = 02/22/15 Pct Recovery = 80% Analysis Date = 02/17/15 Pct Recovery = 80% Analysis Date = 02/17/15 Pct Recovery = 80% Analysis Date = 02/13/15 Pct Recovery = 80% Analysis Date = 02/13/15 Pct Recovery = 80% Analysis Date = 02/08/15 Pct Recovery = 80% Analysis Date = 02/08/15 Pct Recovery = 80% Analysis Date = 02/04/15 Pct Recovery = 81% Analysis Date = 02/04/15 Pct Recovery = 81% Analysis Date = 01/30/15 Pct Recovery = 81% Analysis Date = 01/30/15 Pct Recovery = 81% Analysis Date = 01/25/15 Pct Recovery = 81% Analysis Date = 01/25/15 Pct Recovery = 81% Analysis Date = 01/21/15 Pct Recovery = 81% Analysis Date = 01/21/15 Pct Recovery = 81% Analysis Date = 01/16/15 Pct Recovery = 82% Analysis Date = 01/16/15 Pct Recovery = 82% Analysis Date = 01/12/15 Pct Recovery = 82% Analysis Date = 01/12/15 Pct Recovery = 82% Analysis Date = 01/07/15 Pct Recovery = 82% Analysis Date = 01/07/15 Pct Recovery = 82% Analysis Date = 01/03/15 Pct Recovery = 82% Analysis Date = 01/03/15 Pct Recovery = 82% Analysis Date = 12/29/14 Pct Recovery = 83% Analysis Date = 12/29/14 Pct Recovery = 83% Analysis Date = 12/25/14 Pct Recovery = 83% Analysis Date = 12/25/14 Pct Recovery = 83% Analysis Date = 12/20/14 Pct Recovery = 83% Analysis Date = 12/20/14 Pct Recovery = 83% Analysis Date = 12/16/14 Pct Recovery = 83% Analysis Date = 12/16/14 Pct Recovery = 83% Analysis Date = 12/11/14 Pct Recovery = 84% Analysis Date = 12/11/14 Pct Recovery = 84% Analysis Date = 12/06/14 Pct Recovery = 84% Analysis Date = 12/06/14 Pct Recovery = 84% Analysis Date = 12/02/14 Pct Recovery = 84% Analysis Date = 12/02/14 Pct Recovery = 84% Analysis Date = 11/27/14 Pct Recovery = 84% Analysis Date = 11/27/14 Pct Recovery = 84% Analysis Date = 11/23/14 Pct Recovery = 84% Analysis Date = 11/23/14 Pct Recovery = 84% Analysis Date = 11/18/14 Pct Recovery = 84% Analysis Date = 11/18/14 Pct Recovery = 84% Analysis Date = 11/14/14 Pct Recovery = 85% Analysis Date = 11/14/14 Pct Recovery = 85% Analysis Date = 11/09/14 Pct Recovery = 85% Analysis Date = 11/09/14 Pct Recovery = 85% Analysis Date = 11/05/14 Pct Recovery = 85% Analysis Date = 11/05/14 Pct Recovery = 85% Analysis Date = 10/31/14 Pct Recovery = 85% Analysis Date = 10/31/14 Pct Recovery = 85% Analysis Date = 10/27/14 Pct Recovery = 85% Analysis Date = 10/27/14 Pct Recovery = 85% Analysis Date = 10/22/14 Pct Recovery = 85% Analysis Date = 10/22/14 Pct Recovery = 85% Analysis Date = 10/18/14 Pct Recovery = 85% Analysis Date = 10/18/14 Pct Recovery = 85% Analysis Date = 10/13/14 Pct Recovery = 85% Analysis Date = 10/13/14 Pct Recovery = 85% Analysis Date = 10/08/14 Pct Recovery = 85% Analysis Date = 10/08/14 Pct Recovery = 85% Analysis Date = 10/04/14 Pct Recovery = 85% Analysis Date = 10/04/14 Pct Recovery = 85% Analysis Date = 09/29/14 Pct Recovery = 86% Analysis Date = 09/29/14 Pct Recovery = 86% Analysis Date = 09/25/14 Pct Recovery = 86% Analysis Date = 09/25/14 Pct Recovery = 86% Analysis Date = 09/20/14 Pct Recovery = 86% Analysis Date = 09/20/14 Pct Recovery = 86% Analysis Date = 09/16/14 Pct Recovery = 86% Analysis Date = 09/16/14 Pct Recovery = 86% Analysis Date = 09/11/14 Pct Recovery = 86% Analysis Date = 09/11/14 Pct Recovery = 86% Analysis Date = 09/07/14 Pct Recovery = 86% Analysis Date = 09/07/14 Pct Recovery = 86% Analysis Date = 09/02/14 Pct Recovery = 86% Analysis Date = 09/02/14 Pct Recovery = 86% Analysis Date = 08/29/14 Pct Recovery = 86% Analysis Date = 08/29/14 Pct Recovery = 86% Analysis Date = 08/24/14 Pct Recovery = 86% Analysis Date = 08/24/14 Pct Recovery = 86% Analysis Date = 08/20/14 Pct Recovery = 86% Analysis Date = 08/20/14 Pct Recovery = 86% Analysis Date = 08/15/14 Pct Recovery = 86% Analysis Date = 08/15/14 Pct Recovery = 86% Analysis Date = 08/10/14 Pct Recovery = 86% Analysis Date = 08/10/14 Pct Recovery = 86% Analysis Date = 08/06/14 Pct Recovery = 86% Analysis Date = 08/06/14 Pct Recovery = 86% Analysis Date = 08/01/14 Pct Recovery = 86% Analysis Date = 08/01/14 Pct Recovery = 86% Analysis Date = 07/28/14 Pct Recovery = 86% Analysis Date = 07/28/14 Pct Recovery = 86% Analysis Date = 07/23/14 Pct Recovery = 86% Analysis Date = 07/23/14 Pct Recovery = 86% Analysis Date = 07/19/14 Pct Recovery = 86% Analysis Date = 07/19/14 Pct Recovery = 86% Analysis Date = 07/14/14 Pct Recovery = 86% Analysis Date = 07/14/14 Pct Recovery = 86% Analysis Date = 07/10/14 Pct Recovery = 86% Analysis Date = 07/10/14 Pct Recovery = 86% Analysis Date = 07/05/14 Pct Recovery = 86% Analysis Date = 07/05/14 Pct Recovery = 86% Analysis Date = 07/01/14 Pct Recovery = 86% Analysis Date = 07/01/14 Pct Recovery = 86% Analysis Date = 06/26/14 Pct Recovery = 86% Analysis Date = 06/26/14 Pct Recovery = 86% Analysis Date = 06/22/14 Pct Recovery = 86% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
FAMOTIDINE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 2 62% 4% 62% 4%
>= Reporting Level 39 55% 56% 45% 35%
Total 41 55% 55% 45% 35%

Sample Statistics
FAMOTIDINE

Characteristic N % % Basis
Plotted 41 55% Spiked
Estimated Values 41 55% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 13 17% Spiked
Spiked 75 .  
False Negatives 21 28% 21 out of 75
Not Spiked 40 .  
False Positives 0 0% 0 out of 40

BQS OBSP Determination:
FENOFIBRATE
METHOD: 2440 , TESTIDCODE: 67489LCM56
Open Data Set

Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 58% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 60% Analysis Date = 11/04/15 SpikeMix = Abs 052215: 80 µl & Abs 050115: 80 µl Pct Recovery = 58% Analysis Date = 01/17/16 SpikeMix = ERA 0406-15-09: 80 µl & ERA 0406-15-07A: 80 µl Pct Recovery = 25% Analysis Date = 11/24/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 53% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 31% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 22% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 38% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 39% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 50% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-04: 15 µl & Abs 041814: 15 µl Pct Recovery = 27% Analysis Date = 12/06/14 SpikeMix = ERA 0318-14-02: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 34% Analysis Date = 10/25/14 SpikeMix = Abs 041614: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 24% Analysis Date = 10/11/14 SpikeMix = ERA 0318-14-02: 60 µl & ERA 0319-14-04: 60 µl Pct Recovery = 32% Analysis Date = 05/07/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 59% Analysis Date = 01/16/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 60% Analysis Date = 12/06/14 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 43% Analysis Date = 08/21/14 SpikeMix = ERA 0318-14-02: 60 µl & Abs 041714: 60 µl Pct Recovery = 40% Analysis Date = 07/12/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 46% Analysis Date = 06/11/14 SpikeMix = Abs 041614: 60 µl & Abs 041714: 60 µl Pct Recovery = 64% Analysis Date = 05/21/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 49% Analysis Date = 02/23/16 SpikeMix = Abs 052215: 40 µl & Abs 050115: 40 µl Pct Recovery = 114% Analysis Date = 09/10/15 SpikeMix = Abs 052215: 40 µl & ERA 0406-15-07A: 40 µl Pct Recovery = 64% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-08: 40 µl & ERA 0406-15-09: 40 µl Pct Recovery = 67% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 24% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 31% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 23% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 63% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 86% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 68% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 62% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 44% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 41% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 43% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 51% Analysis Date = 02/10/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 57% Analysis Date = 12/07/14 SpikeMix = ERA 0318-14-02: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 36% Analysis Date = 10/11/14 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 15% Analysis Date = 10/10/14 SpikeMix = Abs 041714: 30 µl & Abs 041814: 30 µl Pct Recovery = 34% Analysis Date = 11/24/15 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 72% Analysis Date = 09/09/15 SpikeMix = ERA 0406-15-08: 20 µl & Abs 052215: 20 µl Pct Recovery = 62% Analysis Date = 06/26/15 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 109% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-08: 20 µl & ERA 0406-15-09: 20 µl Pct Recovery = 18% Analysis Date = 11/24/15 SpikeMix = ERA 0406-15-09: 20 µl & Abs 050115: 20 µl Pct Recovery = 63% Analysis Date = 01/18/17 Pct Recovery = 53% Analysis Date = 01/14/17 Pct Recovery = 53% Analysis Date = 01/14/17 Pct Recovery = 53% Analysis Date = 01/09/17 Pct Recovery = 52% Analysis Date = 01/09/17 Pct Recovery = 52% Analysis Date = 01/04/17 Pct Recovery = 52% Analysis Date = 01/04/17 Pct Recovery = 52% Analysis Date = 12/30/16 Pct Recovery = 52% Analysis Date = 12/30/16 Pct Recovery = 52% Analysis Date = 12/25/16 Pct Recovery = 51% Analysis Date = 12/25/16 Pct Recovery = 51% Analysis Date = 12/20/16 Pct Recovery = 51% Analysis Date = 12/20/16 Pct Recovery = 51% Analysis Date = 12/15/16 Pct Recovery = 51% Analysis Date = 12/15/16 Pct Recovery = 51% Analysis Date = 12/11/16 Pct Recovery = 51% Analysis Date = 12/11/16 Pct Recovery = 51% Analysis Date = 12/06/16 Pct Recovery = 50% Analysis Date = 12/06/16 Pct Recovery = 50% Analysis Date = 12/01/16 Pct Recovery = 50% Analysis Date = 12/01/16 Pct Recovery = 50% Analysis Date = 11/26/16 Pct Recovery = 50% Analysis Date = 11/26/16 Pct Recovery = 50% Analysis Date = 11/21/16 Pct Recovery = 50% Analysis Date = 11/21/16 Pct Recovery = 50% Analysis Date = 11/16/16 Pct Recovery = 49% Analysis Date = 11/16/16 Pct Recovery = 49% Analysis Date = 11/11/16 Pct Recovery = 49% Analysis Date = 11/11/16 Pct Recovery = 49% Analysis Date = 11/06/16 Pct Recovery = 49% Analysis Date = 11/06/16 Pct Recovery = 49% Analysis Date = 11/02/16 Pct Recovery = 49% Analysis Date = 11/02/16 Pct Recovery = 49% Analysis Date = 10/28/16 Pct Recovery = 48% Analysis Date = 10/28/16 Pct Recovery = 48% Analysis Date = 10/23/16 Pct Recovery = 48% Analysis Date = 10/23/16 Pct Recovery = 48% Analysis Date = 10/18/16 Pct Recovery = 48% Analysis Date = 10/18/16 Pct Recovery = 48% Analysis Date = 10/13/16 Pct Recovery = 48% Analysis Date = 10/13/16 Pct Recovery = 48% Analysis Date = 10/08/16 Pct Recovery = 48% Analysis Date = 10/08/16 Pct Recovery = 48% Analysis Date = 10/03/16 Pct Recovery = 48% Analysis Date = 10/03/16 Pct Recovery = 48% Analysis Date = 09/28/16 Pct Recovery = 48% Analysis Date = 09/28/16 Pct Recovery = 48% Analysis Date = 09/24/16 Pct Recovery = 47% Analysis Date = 09/24/16 Pct Recovery = 47% Analysis Date = 09/19/16 Pct Recovery = 47% Analysis Date = 09/19/16 Pct Recovery = 47% Analysis Date = 09/14/16 Pct Recovery = 47% Analysis Date = 09/14/16 Pct Recovery = 47% Analysis Date = 09/09/16 Pct Recovery = 47% Analysis Date = 09/09/16 Pct Recovery = 47% Analysis Date = 09/04/16 Pct Recovery = 47% Analysis Date = 09/04/16 Pct Recovery = 47% Analysis Date = 08/30/16 Pct Recovery = 47% Analysis Date = 08/30/16 Pct Recovery = 47% Analysis Date = 08/25/16 Pct Recovery = 47% Analysis Date = 08/25/16 Pct Recovery = 47% Analysis Date = 08/21/16 Pct Recovery = 47% Analysis Date = 08/21/16 Pct Recovery = 47% Analysis Date = 08/16/16 Pct Recovery = 47% Analysis Date = 08/16/16 Pct Recovery = 47% Analysis Date = 08/11/16 Pct Recovery = 47% Analysis Date = 08/11/16 Pct Recovery = 47% Analysis Date = 08/06/16 Pct Recovery = 47% Analysis Date = 08/06/16 Pct Recovery = 47% Analysis Date = 08/01/16 Pct Recovery = 47% Analysis Date = 08/01/16 Pct Recovery = 47% Analysis Date = 07/27/16 Pct Recovery = 47% Analysis Date = 07/27/16 Pct Recovery = 47% Analysis Date = 07/22/16 Pct Recovery = 47% Analysis Date = 07/22/16 Pct Recovery = 47% Analysis Date = 07/17/16 Pct Recovery = 47% Analysis Date = 07/17/16 Pct Recovery = 47% Analysis Date = 07/13/16 Pct Recovery = 48% Analysis Date = 07/13/16 Pct Recovery = 48% Analysis Date = 07/08/16 Pct Recovery = 48% Analysis Date = 07/08/16 Pct Recovery = 48% Analysis Date = 07/03/16 Pct Recovery = 48% Analysis Date = 07/03/16 Pct Recovery = 48% Analysis Date = 06/28/16 Pct Recovery = 48% Analysis Date = 06/28/16 Pct Recovery = 48% Analysis Date = 06/23/16 Pct Recovery = 49% Analysis Date = 06/23/16 Pct Recovery = 49% Analysis Date = 06/18/16 Pct Recovery = 49% Analysis Date = 06/18/16 Pct Recovery = 49% Analysis Date = 06/13/16 Pct Recovery = 49% Analysis Date = 06/13/16 Pct Recovery = 49% Analysis Date = 06/08/16 Pct Recovery = 49% Analysis Date = 06/08/16 Pct Recovery = 49% Analysis Date = 06/04/16 Pct Recovery = 50% Analysis Date = 06/04/16 Pct Recovery = 50% Analysis Date = 05/30/16 Pct Recovery = 50% Analysis Date = 05/30/16 Pct Recovery = 50% Analysis Date = 05/25/16 Pct Recovery = 50% Analysis Date = 05/25/16 Pct Recovery = 50% Analysis Date = 05/20/16 Pct Recovery = 50% Analysis Date = 05/20/16 Pct Recovery = 50% Analysis Date = 05/15/16 Pct Recovery = 51% Analysis Date = 05/15/16 Pct Recovery = 51% Analysis Date = 05/10/16 Pct Recovery = 51% Analysis Date = 05/10/16 Pct Recovery = 51% Analysis Date = 05/05/16 Pct Recovery = 51% Analysis Date = 05/05/16 Pct Recovery = 51% Analysis Date = 05/01/16 Pct Recovery = 51% Analysis Date = 05/01/16 Pct Recovery = 51% Analysis Date = 04/26/16 Pct Recovery = 52% Analysis Date = 04/26/16 Pct Recovery = 52% Analysis Date = 04/21/16 Pct Recovery = 52% Analysis Date = 04/21/16 Pct Recovery = 52% Analysis Date = 04/16/16 Pct Recovery = 52% Analysis Date = 04/16/16 Pct Recovery = 52% Analysis Date = 04/11/16 Pct Recovery = 52% Analysis Date = 04/11/16 Pct Recovery = 52% Analysis Date = 04/06/16 Pct Recovery = 53% Analysis Date = 04/06/16 Pct Recovery = 53% Analysis Date = 04/01/16 Pct Recovery = 53% Analysis Date = 04/01/16 Pct Recovery = 53% Analysis Date = 03/27/16 Pct Recovery = 53% Analysis Date = 03/27/16 Pct Recovery = 53% Analysis Date = 03/23/16 Pct Recovery = 53% Analysis Date = 03/23/16 Pct Recovery = 53% Analysis Date = 03/18/16 Pct Recovery = 54% Analysis Date = 03/18/16 Pct Recovery = 54% Analysis Date = 03/13/16 Pct Recovery = 54% Analysis Date = 03/13/16 Pct Recovery = 54% Analysis Date = 03/08/16 Pct Recovery = 54% Analysis Date = 03/08/16 Pct Recovery = 54% Analysis Date = 03/03/16 Pct Recovery = 54% Analysis Date = 03/03/16 Pct Recovery = 54% Analysis Date = 02/27/16 Pct Recovery = 55% Analysis Date = 02/27/16 Pct Recovery = 55% Analysis Date = 02/22/16 Pct Recovery = 55% Analysis Date = 02/22/16 Pct Recovery = 55% Analysis Date = 02/17/16 Pct Recovery = 55% Analysis Date = 02/17/16 Pct Recovery = 55% Analysis Date = 02/13/16 Pct Recovery = 55% Analysis Date = 02/13/16 Pct Recovery = 55% Analysis Date = 02/08/16 Pct Recovery = 56% Analysis Date = 02/08/16 Pct Recovery = 56% Analysis Date = 02/03/16 Pct Recovery = 56% Analysis Date = 02/03/16 Pct Recovery = 56% Analysis Date = 01/29/16 Pct Recovery = 56% Analysis Date = 01/29/16 Pct Recovery = 56% Analysis Date = 01/24/16 Pct Recovery = 56% Analysis Date = 01/24/16 Pct Recovery = 56% Analysis Date = 01/19/16 Pct Recovery = 57% Analysis Date = 01/19/16 Pct Recovery = 57% Analysis Date = 01/14/16 Pct Recovery = 57% Analysis Date = 01/14/16 Pct Recovery = 57% Analysis Date = 01/10/16 Pct Recovery = 57% Analysis Date = 01/10/16 Pct Recovery = 57% Analysis Date = 01/05/16 Pct Recovery = 57% Analysis Date = 01/05/16 Pct Recovery = 57% Analysis Date = 12/31/15 Pct Recovery = 58% Analysis Date = 12/31/15 Pct Recovery = 58% Analysis Date = 12/26/15 Pct Recovery = 58% Analysis Date = 12/26/15 Pct Recovery = 58% Analysis Date = 12/21/15 Pct Recovery = 58% Analysis Date = 12/21/15 Pct Recovery = 58% Analysis Date = 12/16/15 Pct Recovery = 59% Analysis Date = 12/16/15 Pct Recovery = 59% Analysis Date = 12/11/15 Pct Recovery = 59% Analysis Date = 12/11/15 Pct Recovery = 59% Analysis Date = 12/06/15 Pct Recovery = 59% Analysis Date = 12/06/15 Pct Recovery = 59% Analysis Date = 12/02/15 Pct Recovery = 60% Analysis Date = 12/02/15 Pct Recovery = 60% Analysis Date = 11/27/15 Pct Recovery = 60% Analysis Date = 11/27/15 Pct Recovery = 60% Analysis Date = 11/22/15 Pct Recovery = 60% Analysis Date = 11/22/15 Pct Recovery = 60% Analysis Date = 11/17/15 Pct Recovery = 60% Analysis Date = 11/17/15 Pct Recovery = 60% Analysis Date = 11/12/15 Pct Recovery = 60% Analysis Date = 11/12/15 Pct Recovery = 60% Analysis Date = 11/07/15 Pct Recovery = 60% Analysis Date = 11/07/15 Pct Recovery = 60% Analysis Date = 11/02/15 Pct Recovery = 60% Analysis Date = 11/02/15 Pct Recovery = 60% Analysis Date = 10/28/15 Pct Recovery = 60% Analysis Date = 10/28/15 Pct Recovery = 60% Analysis Date = 10/24/15 Pct Recovery = 60% Analysis Date = 10/24/15 Pct Recovery = 60% Analysis Date = 10/19/15 Pct Recovery = 60% Analysis Date = 10/19/15 Pct Recovery = 60% Analysis Date = 10/14/15 Pct Recovery = 60% Analysis Date = 10/14/15 Pct Recovery = 60% Analysis Date = 10/09/15 Pct Recovery = 60% Analysis Date = 10/09/15 Pct Recovery = 60% Analysis Date = 10/04/15 Pct Recovery = 60% Analysis Date = 10/04/15 Pct Recovery = 60% Analysis Date = 09/29/15 Pct Recovery = 60% Analysis Date = 09/29/15 Pct Recovery = 60% Analysis Date = 09/24/15 Pct Recovery = 60% Analysis Date = 09/24/15 Pct Recovery = 60% Analysis Date = 09/19/15 Pct Recovery = 60% Analysis Date = 09/19/15 Pct Recovery = 60% Analysis Date = 09/15/15 Pct Recovery = 60% Analysis Date = 09/15/15 Pct Recovery = 60% Analysis Date = 09/10/15 Pct Recovery = 60% Analysis Date = 09/10/15 Pct Recovery = 60% Analysis Date = 09/05/15 Pct Recovery = 60% Analysis Date = 09/05/15 Pct Recovery = 60% Analysis Date = 08/31/15 Pct Recovery = 60% Analysis Date = 08/31/15 Pct Recovery = 60% Analysis Date = 08/26/15 Pct Recovery = 60% Analysis Date = 08/26/15 Pct Recovery = 60% Analysis Date = 08/21/15 Pct Recovery = 59% Analysis Date = 08/21/15 Pct Recovery = 59% Analysis Date = 08/16/15 Pct Recovery = 59% Analysis Date = 08/16/15 Pct Recovery = 59% Analysis Date = 08/12/15 Pct Recovery = 59% Analysis Date = 08/12/15 Pct Recovery = 59% Analysis Date = 08/07/15 Pct Recovery = 58% Analysis Date = 08/07/15 Pct Recovery = 58% Analysis Date = 08/02/15 Pct Recovery = 58% Analysis Date = 08/02/15 Pct Recovery = 58% Analysis Date = 07/28/15 Pct Recovery = 58% Analysis Date = 07/28/15 Pct Recovery = 58% Analysis Date = 07/23/15 Pct Recovery = 58% Analysis Date = 07/23/15 Pct Recovery = 58% Analysis Date = 07/18/15 Pct Recovery = 57% Analysis Date = 07/18/15 Pct Recovery = 57% Analysis Date = 07/13/15 Pct Recovery = 57% Analysis Date = 07/13/15 Pct Recovery = 57% Analysis Date = 07/08/15 Pct Recovery = 57% Analysis Date = 07/08/15 Pct Recovery = 57% Analysis Date = 07/04/15 Pct Recovery = 57% Analysis Date = 07/04/15 Pct Recovery = 57% Analysis Date = 06/29/15 Pct Recovery = 56% Analysis Date = 06/29/15 Pct Recovery = 56% Analysis Date = 06/24/15 Pct Recovery = 56% Analysis Date = 06/24/15 Pct Recovery = 56% Analysis Date = 06/19/15 Pct Recovery = 56% Analysis Date = 06/19/15 Pct Recovery = 56% Analysis Date = 06/14/15 Pct Recovery = 55% Analysis Date = 06/14/15 Pct Recovery = 55% Analysis Date = 06/09/15 Pct Recovery = 55% Analysis Date = 06/09/15 Pct Recovery = 55% Analysis Date = 06/04/15 Pct Recovery = 55% Analysis Date = 06/04/15 Pct Recovery = 55% Analysis Date = 05/30/15 Pct Recovery = 55% Analysis Date = 05/30/15 Pct Recovery = 55% Analysis Date = 05/26/15 Pct Recovery = 54% Analysis Date = 05/26/15 Pct Recovery = 54% Analysis Date = 05/21/15 Pct Recovery = 54% Analysis Date = 05/21/15 Pct Recovery = 54% Analysis Date = 05/16/15 Pct Recovery = 54% Analysis Date = 05/16/15 Pct Recovery = 54% Analysis Date = 05/11/15 Pct Recovery = 53% Analysis Date = 05/11/15 Pct Recovery = 53% Analysis Date = 05/06/15 Pct Recovery = 53% Analysis Date = 05/06/15 Pct Recovery = 53% Analysis Date = 05/01/15 Pct Recovery = 53% Analysis Date = 05/01/15 Pct Recovery = 53% Analysis Date = 04/26/15 Pct Recovery = 53% Analysis Date = 04/26/15 Pct Recovery = 53% Analysis Date = 04/22/15 Pct Recovery = 52% Analysis Date = 04/22/15 Pct Recovery = 52% Analysis Date = 04/17/15 Pct Recovery = 52% Analysis Date = 04/17/15 Pct Recovery = 52% Analysis Date = 04/12/15 Pct Recovery = 52% Analysis Date = 04/12/15 Pct Recovery = 52% Analysis Date = 04/07/15 Pct Recovery = 51% Analysis Date = 04/07/15 Pct Recovery = 51% Analysis Date = 04/02/15 Pct Recovery = 51% Analysis Date = 04/02/15 Pct Recovery = 51% Analysis Date = 03/28/15 Pct Recovery = 51% Analysis Date = 03/28/15 Pct Recovery = 51% Analysis Date = 03/23/15 Pct Recovery = 51% Analysis Date = 03/23/15 Pct Recovery = 51% Analysis Date = 03/18/15 Pct Recovery = 50% Analysis Date = 03/18/15 Pct Recovery = 50% Analysis Date = 03/14/15 Pct Recovery = 50% Analysis Date = 03/14/15 Pct Recovery = 50% Analysis Date = 03/09/15 Pct Recovery = 50% Analysis Date = 03/09/15 Pct Recovery = 50% Analysis Date = 03/04/15 Pct Recovery = 50% Analysis Date = 03/04/15 Pct Recovery = 50% Analysis Date = 02/27/15 Pct Recovery = 49% Analysis Date = 02/27/15 Pct Recovery = 49% Analysis Date = 02/22/15 Pct Recovery = 49% Analysis Date = 02/22/15 Pct Recovery = 49% Analysis Date = 02/17/15 Pct Recovery = 49% Analysis Date = 02/17/15 Pct Recovery = 49% Analysis Date = 02/12/15 Pct Recovery = 48% Analysis Date = 02/12/15 Pct Recovery = 48% Analysis Date = 02/07/15 Pct Recovery = 48% Analysis Date = 02/07/15 Pct Recovery = 48% Analysis Date = 02/03/15 Pct Recovery = 48% Analysis Date = 02/03/15 Pct Recovery = 48% Analysis Date = 01/29/15 Pct Recovery = 48% Analysis Date = 01/29/15 Pct Recovery = 48% Analysis Date = 01/24/15 Pct Recovery = 47% Analysis Date = 01/24/15 Pct Recovery = 47% Analysis Date = 01/19/15 Pct Recovery = 47% Analysis Date = 01/19/15 Pct Recovery = 47% Analysis Date = 01/14/15 Pct Recovery = 47% Analysis Date = 01/14/15 Pct Recovery = 47% Analysis Date = 01/09/15 Pct Recovery = 47% Analysis Date = 01/09/15 Pct Recovery = 47% Analysis Date = 01/04/15 Pct Recovery = 46% Analysis Date = 01/04/15 Pct Recovery = 46% Analysis Date = 12/31/14 Pct Recovery = 46% Analysis Date = 12/31/14 Pct Recovery = 46% Analysis Date = 12/26/14 Pct Recovery = 46% Analysis Date = 12/26/14 Pct Recovery = 46% Analysis Date = 12/21/14 Pct Recovery = 46% Analysis Date = 12/21/14 Pct Recovery = 46% Analysis Date = 12/16/14 Pct Recovery = 45% Analysis Date = 12/16/14 Pct Recovery = 45% Analysis Date = 12/11/14 Pct Recovery = 45% Analysis Date = 12/11/14 Pct Recovery = 45% Analysis Date = 12/06/14 Pct Recovery = 45% Analysis Date = 12/06/14 Pct Recovery = 45% Analysis Date = 12/01/14 Pct Recovery = 45% Analysis Date = 12/01/14 Pct Recovery = 45% Analysis Date = 11/26/14 Pct Recovery = 44% Analysis Date = 11/26/14 Pct Recovery = 44% Analysis Date = 11/22/14 Pct Recovery = 44% Analysis Date = 11/22/14 Pct Recovery = 44% Analysis Date = 11/17/14 Pct Recovery = 44% Analysis Date = 11/17/14 Pct Recovery = 44% Analysis Date = 11/12/14 Pct Recovery = 44% Analysis Date = 11/12/14 Pct Recovery = 44% Analysis Date = 11/07/14 Pct Recovery = 43% Analysis Date = 11/07/14 Pct Recovery = 43% Analysis Date = 11/02/14 Pct Recovery = 43% Analysis Date = 11/02/14 Pct Recovery = 43% Analysis Date = 10/28/14 Pct Recovery = 43% Analysis Date = 10/28/14 Pct Recovery = 43% Analysis Date = 10/23/14 Pct Recovery = 43% Analysis Date = 10/23/14 Pct Recovery = 43% Analysis Date = 10/18/14 Pct Recovery = 42% Analysis Date = 10/18/14 Pct Recovery = 42% Analysis Date = 10/14/14 Pct Recovery = 42% Analysis Date = 10/14/14 Pct Recovery = 42% Analysis Date = 10/09/14 Pct Recovery = 42% Analysis Date = 10/09/14 Pct Recovery = 42% Analysis Date = 10/04/14 Pct Recovery = 42% Analysis Date = 10/04/14 Pct Recovery = 42% Analysis Date = 09/29/14 Pct Recovery = 41% Analysis Date = 09/29/14 Pct Recovery = 41% Analysis Date = 09/24/14 Pct Recovery = 41% Analysis Date = 09/24/14 Pct Recovery = 41% Analysis Date = 09/19/14 Pct Recovery = 41% Analysis Date = 09/19/14 Pct Recovery = 41% Analysis Date = 09/14/14 Pct Recovery = 41% Analysis Date = 09/14/14 Pct Recovery = 41% Analysis Date = 09/10/14 Pct Recovery = 40% Analysis Date = 09/10/14 Pct Recovery = 40% Analysis Date = 09/05/14 Pct Recovery = 40% Analysis Date = 09/05/14 Pct Recovery = 40% Analysis Date = 08/31/14 Pct Recovery = 40% Analysis Date = 08/31/14 Pct Recovery = 40% Analysis Date = 08/26/14 Pct Recovery = 40% Analysis Date = 08/26/14 Pct Recovery = 40% Analysis Date = 08/21/14 Pct Recovery = 39% Analysis Date = 08/21/14 Pct Recovery = 39% Analysis Date = 08/16/14 Pct Recovery = 39% Analysis Date = 08/16/14 Pct Recovery = 39% Analysis Date = 08/11/14 Pct Recovery = 39% Analysis Date = 08/11/14 Pct Recovery = 39% Analysis Date = 08/06/14 Pct Recovery = 39% Analysis Date = 08/06/14 Pct Recovery = 39% Analysis Date = 08/02/14 Pct Recovery = 39% Analysis Date = 08/02/14 Pct Recovery = 39% Analysis Date = 07/28/14 Pct Recovery = 38% Analysis Date = 07/28/14 Pct Recovery = 38% Analysis Date = 07/23/14 Pct Recovery = 38% Analysis Date = 07/23/14 Pct Recovery = 38% Analysis Date = 07/18/14 Pct Recovery = 38% Analysis Date = 07/18/14 Pct Recovery = 38% Analysis Date = 07/13/14 Pct Recovery = 38% Analysis Date = 07/13/14 Pct Recovery = 38% Analysis Date = 07/08/14 Pct Recovery = 37% Analysis Date = 07/08/14 Pct Recovery = 37% Analysis Date = 07/03/14 Pct Recovery = 37% Analysis Date = 07/03/14 Pct Recovery = 37% Analysis Date = 06/28/14 Pct Recovery = 37% Analysis Date = 06/28/14 Pct Recovery = 37% Analysis Date = 06/24/14 Pct Recovery = 37% Analysis Date = 06/24/14 Pct Recovery = 37% Analysis Date = 06/19/14 Pct Recovery = 37% Analysis Date = 06/19/14 Pct Recovery = 37% Analysis Date = 06/14/14 Pct Recovery = 36% Analysis Date = 06/14/14 Pct Recovery = 36% Analysis Date = 06/09/14 Pct Recovery = 36% Analysis Date = 06/09/14 Pct Recovery = 36% Analysis Date = 06/04/14 Pct Recovery = 36% Analysis Date = 06/04/14 Pct Recovery = 36% Analysis Date = 05/30/14 Pct Recovery = 36% Analysis Date = 05/30/14 Pct Recovery = 36% Analysis Date = 05/25/14 Pct Recovery = 36% Analysis Date = 05/25/14 Pct Recovery = 36% Analysis Date = 05/21/14 Pct Recovery = 36% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
FENOFIBRATE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 44 49% 22% 47% 21%
Total 44 49% 22% 47% 21%

Sample Statistics
FENOFIBRATE

Characteristic N % % Basis
Plotted 44 57% Spiked
Estimated Values 31 40% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 6 8% Spiked
Spiked 77 .  
False Negatives 27 35% 27 out of 77
Not Spiked 38 .  
False Positives 0 0% 0 out of 38

BQS OBSP Determination:
FEXOFENADINE
METHOD: 2440 , TESTIDCODE: 67510LCM56
Open Data Set

Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 64% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 66% Analysis Date = 01/17/16 SpikeMix = ERA 0406-15-09: 80 µl & ERA 0406-15-07A: 80 µl Pct Recovery = 61% Analysis Date = 11/24/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 58% Analysis Date = 11/05/15 SpikeMix = ERA 0406-15-08: 80 µl & Abs 052215: 80 µl Pct Recovery = 62% Analysis Date = 11/04/15 SpikeMix = Abs 052215: 80 µl & Abs 050115: 80 µl Pct Recovery = 73% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 64% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 68% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 78% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 75% Analysis Date = 11/18/16 SpikeMix = ERA 04281604: 80 µl & ERA 04281603: 80 µl Pct Recovery = 61% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & ERA 04281604: 80 µl Pct Recovery = 61% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 53% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 54% Analysis Date = 04/29/15 SpikeMix = ERA 0319-14-05: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 49% Analysis Date = 03/11/15 SpikeMix = ERA 0318-14-02: 15 µl & Abs 041714: 15 µl Pct Recovery = 68% Analysis Date = 02/06/15 SpikeMix = Abs 041814: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 64% Analysis Date = 12/06/14 SpikeMix = ERA 0318-14-02: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 60% Analysis Date = 10/11/14 SpikeMix = ERA 0318-14-02: 60 µl & ERA 0319-14-04: 60 µl Pct Recovery = 50% Analysis Date = 08/21/14 SpikeMix = ERA 0318-14-02: 60 µl & Abs 041714: 60 µl Pct Recovery = 60% Analysis Date = 07/26/14 SpikeMix = ERA 0319-14-05: 60 µl & ERA 0318-14-02: 60 µl Pct Recovery = 70% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 57% Analysis Date = 12/07/14 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 56% Analysis Date = 10/25/14 SpikeMix = Abs 041614: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 56% Analysis Date = 06/22/14 SpikeMix = Abs 041814: 60 µl & Abs 041614: 60 µl Pct Recovery = 87% Analysis Date = 06/11/14 SpikeMix = Abs 041614: 60 µl & Abs 041714: 60 µl Pct Recovery = 73% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-08: 40 µl & ERA 0406-15-09: 40 µl Pct Recovery = 60% Analysis Date = 07/31/15 SpikeMix = ERA 0406-15-09: 40 µl & Abs 050115: 40 µl Pct Recovery = 67% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-08: 40 µl & Abs 052215: 40 µl Pct Recovery = 67% Analysis Date = 02/23/16 SpikeMix = Abs 052215: 40 µl & Abs 050115: 40 µl Pct Recovery = 62% Analysis Date = 09/10/15 SpikeMix = Abs 052215: 40 µl & ERA 0406-15-07A: 40 µl Pct Recovery = 68% Analysis Date = 07/31/15 SpikeMix = Abs 051315: 40 µl & Abs 052215: 40 µl Pct Recovery = 52% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 72% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 66% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 60% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 62% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 68% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 63% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 49% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 48% Analysis Date = 12/07/14 SpikeMix = ERA 0318-14-02: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 56% Analysis Date = 11/04/14 SpikeMix = Abs 041814: 8 µl & ERA 0318-14-02: 8 µl Pct Recovery = 61% Analysis Date = 04/30/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 47% Analysis Date = 02/10/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 62% Analysis Date = 10/24/14 SpikeMix = ERA 0319-14-05: 8 µl & Abs 041614: 8 µl Pct Recovery = 61% Analysis Date = 10/10/14 SpikeMix = Abs 041814: 30 µl & ERA 0318-14-02: 30 µl Pct Recovery = 44% Analysis Date = 08/30/14 SpikeMix = ERA 0318-14-02: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 59% Analysis Date = 07/20/14 SpikeMix = ERA 0318-14-02: 30 µl & Abs 041714: 30 µl Pct Recovery = 57% Analysis Date = 04/23/14 SpikeMix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.2: 20 µl Pct Recovery = 59% Analysis Date = 09/12/14 SpikeMix = Abs 041614: 30 µl & ERA 0319-14-04: 30 µl Pct Recovery = 61% Analysis Date = 07/13/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 67% Analysis Date = 06/28/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 65% Analysis Date = 05/30/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 66% Analysis Date = 05/17/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 77% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 31% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-08: 20 µl & ERA 0406-15-09: 20 µl Pct Recovery = 48% Analysis Date = 11/24/15 SpikeMix = ERA 0406-15-09: 20 µl & Abs 050115: 20 µl Pct Recovery = 64% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 51% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 45% Analysis Date = 02/23/16 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 74% Analysis Date = 11/24/15 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 69% Analysis Date = 09/09/15 SpikeMix = ERA 0406-15-08: 20 µl & Abs 052215: 20 µl Pct Recovery = 67% Analysis Date = 08/27/15 SpikeMix = Abs 052215: 20 µl & Abs 050115: 20 µl Pct Recovery = 57% Analysis Date = 07/09/15 SpikeMix = Abs 050115: 20 µl & Abs 052215: 20 µl Pct Recovery = 60% Analysis Date = 06/26/15 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 56% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 83% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 100% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 71% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 72% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 62% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 60% Analysis Date = 04/09/16 SpikeMix = Abs 051315: 10 µl & ERA 0406-15-09: 10 µl Pct Recovery = 51% Analysis Date = 01/18/17 Pct Recovery = 69% Analysis Date = 01/13/17 Pct Recovery = 69% Analysis Date = 01/13/17 Pct Recovery = 69% Analysis Date = 01/08/17 Pct Recovery = 69% Analysis Date = 01/08/17 Pct Recovery = 69% Analysis Date = 01/03/17 Pct Recovery = 68% Analysis Date = 01/03/17 Pct Recovery = 68% Analysis Date = 12/29/16 Pct Recovery = 68% Analysis Date = 12/29/16 Pct Recovery = 68% Analysis Date = 12/24/16 Pct Recovery = 68% Analysis Date = 12/24/16 Pct Recovery = 68% Analysis Date = 12/19/16 Pct Recovery = 68% Analysis Date = 12/19/16 Pct Recovery = 68% Analysis Date = 12/14/16 Pct Recovery = 68% Analysis Date = 12/14/16 Pct Recovery = 68% Analysis Date = 12/09/16 Pct Recovery = 67% Analysis Date = 12/09/16 Pct Recovery = 67% Analysis Date = 12/04/16 Pct Recovery = 67% Analysis Date = 12/04/16 Pct Recovery = 67% Analysis Date = 11/29/16 Pct Recovery = 67% Analysis Date = 11/29/16 Pct Recovery = 67% Analysis Date = 11/24/16 Pct Recovery = 67% Analysis Date = 11/24/16 Pct Recovery = 67% Analysis Date = 11/19/16 Pct Recovery = 67% Analysis Date = 11/19/16 Pct Recovery = 67% Analysis Date = 11/14/16 Pct Recovery = 66% Analysis Date = 11/14/16 Pct Recovery = 66% Analysis Date = 11/09/16 Pct Recovery = 66% Analysis Date = 11/09/16 Pct Recovery = 66% Analysis Date = 11/04/16 Pct Recovery = 66% Analysis Date = 11/04/16 Pct Recovery = 66% Analysis Date = 10/30/16 Pct Recovery = 66% Analysis Date = 10/30/16 Pct Recovery = 66% Analysis Date = 10/25/16 Pct Recovery = 66% Analysis Date = 10/25/16 Pct Recovery = 66% Analysis Date = 10/20/16 Pct Recovery = 66% Analysis Date = 10/20/16 Pct Recovery = 66% Analysis Date = 10/15/16 Pct Recovery = 65% Analysis Date = 10/15/16 Pct Recovery = 65% Analysis Date = 10/10/16 Pct Recovery = 65% Analysis Date = 10/10/16 Pct Recovery = 65% Analysis Date = 10/05/16 Pct Recovery = 65% Analysis Date = 10/05/16 Pct Recovery = 65% Analysis Date = 09/30/16 Pct Recovery = 65% Analysis Date = 09/30/16 Pct Recovery = 65% Analysis Date = 09/25/16 Pct Recovery = 65% Analysis Date = 09/25/16 Pct Recovery = 65% Analysis Date = 09/20/16 Pct Recovery = 64% Analysis Date = 09/20/16 Pct Recovery = 64% Analysis Date = 09/15/16 Pct Recovery = 64% Analysis Date = 09/15/16 Pct Recovery = 64% Analysis Date = 09/10/16 Pct Recovery = 64% Analysis Date = 09/10/16 Pct Recovery = 64% Analysis Date = 09/05/16 Pct Recovery = 64% Analysis Date = 09/05/16 Pct Recovery = 64% Analysis Date = 08/31/16 Pct Recovery = 64% Analysis Date = 08/31/16 Pct Recovery = 64% Analysis Date = 08/26/16 Pct Recovery = 64% Analysis Date = 08/26/16 Pct Recovery = 64% Analysis Date = 08/21/16 Pct Recovery = 63% Analysis Date = 08/21/16 Pct Recovery = 63% Analysis Date = 08/16/16 Pct Recovery = 63% Analysis Date = 08/16/16 Pct Recovery = 63% Analysis Date = 08/11/16 Pct Recovery = 63% Analysis Date = 08/11/16 Pct Recovery = 63% Analysis Date = 08/06/16 Pct Recovery = 63% Analysis Date = 08/06/16 Pct Recovery = 63% Analysis Date = 08/01/16 Pct Recovery = 63% Analysis Date = 08/01/16 Pct Recovery = 63% Analysis Date = 07/27/16 Pct Recovery = 63% Analysis Date = 07/27/16 Pct Recovery = 63% Analysis Date = 07/22/16 Pct Recovery = 62% Analysis Date = 07/22/16 Pct Recovery = 62% Analysis Date = 07/17/16 Pct Recovery = 62% Analysis Date = 07/17/16 Pct Recovery = 62% Analysis Date = 07/12/16 Pct Recovery = 62% Analysis Date = 07/12/16 Pct Recovery = 62% Analysis Date = 07/07/16 Pct Recovery = 62% Analysis Date = 07/07/16 Pct Recovery = 62% Analysis Date = 07/02/16 Pct Recovery = 62% Analysis Date = 07/02/16 Pct Recovery = 62% Analysis Date = 06/27/16 Pct Recovery = 62% Analysis Date = 06/27/16 Pct Recovery = 62% Analysis Date = 06/22/16 Pct Recovery = 62% Analysis Date = 06/22/16 Pct Recovery = 62% Analysis Date = 06/17/16 Pct Recovery = 62% Analysis Date = 06/17/16 Pct Recovery = 62% Analysis Date = 06/12/16 Pct Recovery = 62% Analysis Date = 06/12/16 Pct Recovery = 62% Analysis Date = 06/07/16 Pct Recovery = 62% Analysis Date = 06/07/16 Pct Recovery = 62% Analysis Date = 06/02/16 Pct Recovery = 62% Analysis Date = 06/02/16 Pct Recovery = 62% Analysis Date = 05/28/16 Pct Recovery = 62% Analysis Date = 05/28/16 Pct Recovery = 62% Analysis Date = 05/23/16 Pct Recovery = 62% Analysis Date = 05/23/16 Pct Recovery = 62% Analysis Date = 05/18/16 Pct Recovery = 62% Analysis Date = 05/18/16 Pct Recovery = 62% Analysis Date = 05/13/16 Pct Recovery = 62% Analysis Date = 05/13/16 Pct Recovery = 62% Analysis Date = 05/08/16 Pct Recovery = 62% Analysis Date = 05/08/16 Pct Recovery = 62% Analysis Date = 05/03/16 Pct Recovery = 61% Analysis Date = 05/03/16 Pct Recovery = 61% Analysis Date = 04/28/16 Pct Recovery = 61% Analysis Date = 04/28/16 Pct Recovery = 61% Analysis Date = 04/23/16 Pct Recovery = 61% Analysis Date = 04/23/16 Pct Recovery = 61% Analysis Date = 04/18/16 Pct Recovery = 61% Analysis Date = 04/18/16 Pct Recovery = 61% Analysis Date = 04/13/16 Pct Recovery = 61% Analysis Date = 04/13/16 Pct Recovery = 61% Analysis Date = 04/08/16 Pct Recovery = 61% Analysis Date = 04/08/16 Pct Recovery = 61% Analysis Date = 04/03/16 Pct Recovery = 61% Analysis Date = 04/03/16 Pct Recovery = 61% Analysis Date = 03/29/16 Pct Recovery = 61% Analysis Date = 03/29/16 Pct Recovery = 61% Analysis Date = 03/24/16 Pct Recovery = 61% Analysis Date = 03/24/16 Pct Recovery = 61% Analysis Date = 03/19/16 Pct Recovery = 61% Analysis Date = 03/19/16 Pct Recovery = 61% Analysis Date = 03/14/16 Pct Recovery = 61% Analysis Date = 03/14/16 Pct Recovery = 61% Analysis Date = 03/09/16 Pct Recovery = 61% Analysis Date = 03/09/16 Pct Recovery = 61% Analysis Date = 03/04/16 Pct Recovery = 61% Analysis Date = 03/04/16 Pct Recovery = 61% Analysis Date = 02/28/16 Pct Recovery = 61% Analysis Date = 02/28/16 Pct Recovery = 61% Analysis Date = 02/23/16 Pct Recovery = 61% Analysis Date = 02/23/16 Pct Recovery = 61% Analysis Date = 02/18/16 Pct Recovery = 61% Analysis Date = 02/18/16 Pct Recovery = 61% Analysis Date = 02/13/16 Pct Recovery = 61% Analysis Date = 02/13/16 Pct Recovery = 61% Analysis Date = 02/08/16 Pct Recovery = 61% Analysis Date = 02/08/16 Pct Recovery = 61% Analysis Date = 02/03/16 Pct Recovery = 60% Analysis Date = 02/03/16 Pct Recovery = 60% Analysis Date = 01/29/16 Pct Recovery = 60% Analysis Date = 01/29/16 Pct Recovery = 60% Analysis Date = 01/24/16 Pct Recovery = 60% Analysis Date = 01/24/16 Pct Recovery = 60% Analysis Date = 01/19/16 Pct Recovery = 60% Analysis Date = 01/19/16 Pct Recovery = 60% Analysis Date = 01/14/16 Pct Recovery = 60% Analysis Date = 01/14/16 Pct Recovery = 60% Analysis Date = 01/09/16 Pct Recovery = 60% Analysis Date = 01/09/16 Pct Recovery = 60% Analysis Date = 01/04/16 Pct Recovery = 60% Analysis Date = 01/04/16 Pct Recovery = 60% Analysis Date = 12/30/15 Pct Recovery = 60% Analysis Date = 12/30/15 Pct Recovery = 60% Analysis Date = 12/25/15 Pct Recovery = 60% Analysis Date = 12/25/15 Pct Recovery = 60% Analysis Date = 12/20/15 Pct Recovery = 60% Analysis Date = 12/20/15 Pct Recovery = 60% Analysis Date = 12/15/15 Pct Recovery = 60% Analysis Date = 12/15/15 Pct Recovery = 60% Analysis Date = 12/10/15 Pct Recovery = 60% Analysis Date = 12/10/15 Pct Recovery = 60% Analysis Date = 12/05/15 Pct Recovery = 60% Analysis Date = 12/05/15 Pct Recovery = 60% Analysis Date = 11/30/15 Pct Recovery = 60% Analysis Date = 11/30/15 Pct Recovery = 60% Analysis Date = 11/25/15 Pct Recovery = 60% Analysis Date = 11/25/15 Pct Recovery = 60% Analysis Date = 11/20/15 Pct Recovery = 60% Analysis Date = 11/20/15 Pct Recovery = 60% Analysis Date = 11/15/15 Pct Recovery = 60% Analysis Date = 11/15/15 Pct Recovery = 60% Analysis Date = 11/10/15 Pct Recovery = 60% Analysis Date = 11/10/15 Pct Recovery = 60% Analysis Date = 11/05/15 Pct Recovery = 60% Analysis Date = 11/05/15 Pct Recovery = 60% Analysis Date = 10/31/15 Pct Recovery = 60% Analysis Date = 10/31/15 Pct Recovery = 60% Analysis Date = 10/26/15 Pct Recovery = 60% Analysis Date = 10/26/15 Pct Recovery = 60% Analysis Date = 10/21/15 Pct Recovery = 60% Analysis Date = 10/21/15 Pct Recovery = 60% Analysis Date = 10/16/15 Pct Recovery = 60% Analysis Date = 10/16/15 Pct Recovery = 60% Analysis Date = 10/11/15 Pct Recovery = 60% Analysis Date = 10/11/15 Pct Recovery = 60% Analysis Date = 10/06/15 Pct Recovery = 60% Analysis Date = 10/06/15 Pct Recovery = 60% Analysis Date = 10/01/15 Pct Recovery = 60% Analysis Date = 10/01/15 Pct Recovery = 60% Analysis Date = 09/26/15 Pct Recovery = 60% Analysis Date = 09/26/15 Pct Recovery = 60% Analysis Date = 09/21/15 Pct Recovery = 60% Analysis Date = 09/21/15 Pct Recovery = 60% Analysis Date = 09/16/15 Pct Recovery = 60% Analysis Date = 09/16/15 Pct Recovery = 60% Analysis Date = 09/11/15 Pct Recovery = 60% Analysis Date = 09/11/15 Pct Recovery = 60% Analysis Date = 09/05/15 Pct Recovery = 60% Analysis Date = 09/05/15 Pct Recovery = 60% Analysis Date = 08/31/15 Pct Recovery = 60% Analysis Date = 08/31/15 Pct Recovery = 60% Analysis Date = 08/26/15 Pct Recovery = 60% Analysis Date = 08/26/15 Pct Recovery = 60% Analysis Date = 08/21/15 Pct Recovery = 60% Analysis Date = 08/21/15 Pct Recovery = 60% Analysis Date = 08/16/15 Pct Recovery = 60% Analysis Date = 08/16/15 Pct Recovery = 60% Analysis Date = 08/11/15 Pct Recovery = 60% Analysis Date = 08/11/15 Pct Recovery = 60% Analysis Date = 08/06/15 Pct Recovery = 60% Analysis Date = 08/06/15 Pct Recovery = 60% Analysis Date = 08/01/15 Pct Recovery = 60% Analysis Date = 08/01/15 Pct Recovery = 60% Analysis Date = 07/27/15 Pct Recovery = 60% Analysis Date = 07/27/15 Pct Recovery = 60% Analysis Date = 07/22/15 Pct Recovery = 60% Analysis Date = 07/22/15 Pct Recovery = 60% Analysis Date = 07/17/15 Pct Recovery = 60% Analysis Date = 07/17/15 Pct Recovery = 60% Analysis Date = 07/12/15 Pct Recovery = 60% Analysis Date = 07/12/15 Pct Recovery = 60% Analysis Date = 07/07/15 Pct Recovery = 60% Analysis Date = 07/07/15 Pct Recovery = 60% Analysis Date = 07/02/15 Pct Recovery = 60% Analysis Date = 07/02/15 Pct Recovery = 60% Analysis Date = 06/27/15 Pct Recovery = 60% Analysis Date = 06/27/15 Pct Recovery = 60% Analysis Date = 06/22/15 Pct Recovery = 60% Analysis Date = 06/22/15 Pct Recovery = 60% Analysis Date = 06/17/15 Pct Recovery = 60% Analysis Date = 06/17/15 Pct Recovery = 60% Analysis Date = 06/12/15 Pct Recovery = 60% Analysis Date = 06/12/15 Pct Recovery = 60% Analysis Date = 06/07/15 Pct Recovery = 60% Analysis Date = 06/07/15 Pct Recovery = 60% Analysis Date = 06/02/15 Pct Recovery = 60% Analysis Date = 06/02/15 Pct Recovery = 60% Analysis Date = 05/28/15 Pct Recovery = 59% Analysis Date = 05/28/15 Pct Recovery = 59% Analysis Date = 05/23/15 Pct Recovery = 59% Analysis Date = 05/23/15 Pct Recovery = 59% Analysis Date = 05/18/15 Pct Recovery = 59% Analysis Date = 05/18/15 Pct Recovery = 59% Analysis Date = 05/13/15 Pct Recovery = 59% Analysis Date = 05/13/15 Pct Recovery = 59% Analysis Date = 05/08/15 Pct Recovery = 59% Analysis Date = 05/08/15 Pct Recovery = 59% Analysis Date = 05/03/15 Pct Recovery = 59% Analysis Date = 05/03/15 Pct Recovery = 59% Analysis Date = 04/28/15 Pct Recovery = 59% Analysis Date = 04/28/15 Pct Recovery = 59% Analysis Date = 04/23/15 Pct Recovery = 59% Analysis Date = 04/23/15 Pct Recovery = 59% Analysis Date = 04/18/15 Pct Recovery = 59% Analysis Date = 04/18/15 Pct Recovery = 59% Analysis Date = 04/13/15 Pct Recovery = 59% Analysis Date = 04/13/15 Pct Recovery = 59% Analysis Date = 04/08/15 Pct Recovery = 59% Analysis Date = 04/08/15 Pct Recovery = 59% Analysis Date = 04/03/15 Pct Recovery = 59% Analysis Date = 04/03/15 Pct Recovery = 59% Analysis Date = 03/29/15 Pct Recovery = 59% Analysis Date = 03/29/15 Pct Recovery = 59% Analysis Date = 03/24/15 Pct Recovery = 59% Analysis Date = 03/24/15 Pct Recovery = 59% Analysis Date = 03/19/15 Pct Recovery = 59% Analysis Date = 03/19/15 Pct Recovery = 59% Analysis Date = 03/14/15 Pct Recovery = 59% Analysis Date = 03/14/15 Pct Recovery = 59% Analysis Date = 03/09/15 Pct Recovery = 59% Analysis Date = 03/09/15 Pct Recovery = 59% Analysis Date = 03/04/15 Pct Recovery = 59% Analysis Date = 03/04/15 Pct Recovery = 59% Analysis Date = 02/27/15 Pct Recovery = 59% Analysis Date = 02/27/15 Pct Recovery = 59% Analysis Date = 02/22/15 Pct Recovery = 60% Analysis Date = 02/22/15 Pct Recovery = 60% Analysis Date = 02/17/15 Pct Recovery = 60% Analysis Date = 02/17/15 Pct Recovery = 60% Analysis Date = 02/12/15 Pct Recovery = 60% Analysis Date = 02/12/15 Pct Recovery = 60% Analysis Date = 02/07/15 Pct Recovery = 60% Analysis Date = 02/07/15 Pct Recovery = 60% Analysis Date = 02/02/15 Pct Recovery = 60% Analysis Date = 02/02/15 Pct Recovery = 60% Analysis Date = 01/28/15 Pct Recovery = 60% Analysis Date = 01/28/15 Pct Recovery = 60% Analysis Date = 01/23/15 Pct Recovery = 60% Analysis Date = 01/23/15 Pct Recovery = 60% Analysis Date = 01/18/15 Pct Recovery = 60% Analysis Date = 01/18/15 Pct Recovery = 60% Analysis Date = 01/13/15 Pct Recovery = 60% Analysis Date = 01/13/15 Pct Recovery = 60% Analysis Date = 01/08/15 Pct Recovery = 60% Analysis Date = 01/08/15 Pct Recovery = 60% Analysis Date = 01/03/15 Pct Recovery = 60% Analysis Date = 01/03/15 Pct Recovery = 60% Analysis Date = 12/29/14 Pct Recovery = 61% Analysis Date = 12/29/14 Pct Recovery = 61% Analysis Date = 12/24/14 Pct Recovery = 61% Analysis Date = 12/24/14 Pct Recovery = 61% Analysis Date = 12/19/14 Pct Recovery = 61% Analysis Date = 12/19/14 Pct Recovery = 61% Analysis Date = 12/14/14 Pct Recovery = 61% Analysis Date = 12/14/14 Pct Recovery = 61% Analysis Date = 12/09/14 Pct Recovery = 61% Analysis Date = 12/09/14 Pct Recovery = 61% Analysis Date = 12/04/14 Pct Recovery = 61% Analysis Date = 12/04/14 Pct Recovery = 61% Analysis Date = 11/29/14 Pct Recovery = 61% Analysis Date = 11/29/14 Pct Recovery = 61% Analysis Date = 11/24/14 Pct Recovery = 61% Analysis Date = 11/24/14 Pct Recovery = 61% Analysis Date = 11/19/14 Pct Recovery = 61% Analysis Date = 11/19/14 Pct Recovery = 61% Analysis Date = 11/14/14 Pct Recovery = 61% Analysis Date = 11/14/14 Pct Recovery = 61% Analysis Date = 11/09/14 Pct Recovery = 61% Analysis Date = 11/09/14 Pct Recovery = 61% Analysis Date = 11/04/14 Pct Recovery = 62% Analysis Date = 11/04/14 Pct Recovery = 62% Analysis Date = 10/30/14 Pct Recovery = 62% Analysis Date = 10/30/14 Pct Recovery = 62% Analysis Date = 10/25/14 Pct Recovery = 62% Analysis Date = 10/25/14 Pct Recovery = 62% Analysis Date = 10/20/14 Pct Recovery = 62% Analysis Date = 10/20/14 Pct Recovery = 62% Analysis Date = 10/15/14 Pct Recovery = 62% Analysis Date = 10/15/14 Pct Recovery = 62% Analysis Date = 10/10/14 Pct Recovery = 62% Analysis Date = 10/10/14 Pct Recovery = 62% Analysis Date = 10/05/14 Pct Recovery = 62% Analysis Date = 10/05/14 Pct Recovery = 62% Analysis Date = 09/30/14 Pct Recovery = 62% Analysis Date = 09/30/14 Pct Recovery = 62% Analysis Date = 09/25/14 Pct Recovery = 62% Analysis Date = 09/25/14 Pct Recovery = 62% Analysis Date = 09/20/14 Pct Recovery = 62% Analysis Date = 09/20/14 Pct Recovery = 62% Analysis Date = 09/15/14 Pct Recovery = 63% Analysis Date = 09/15/14 Pct Recovery = 63% Analysis Date = 09/10/14 Pct Recovery = 63% Analysis Date = 09/10/14 Pct Recovery = 63% Analysis Date = 09/05/14 Pct Recovery = 63% Analysis Date = 09/05/14 Pct Recovery = 63% Analysis Date = 08/31/14 Pct Recovery = 63% Analysis Date = 08/31/14 Pct Recovery = 63% Analysis Date = 08/26/14 Pct Recovery = 63% Analysis Date = 08/26/14 Pct Recovery = 63% Analysis Date = 08/21/14 Pct Recovery = 63% Analysis Date = 08/21/14 Pct Recovery = 63% Analysis Date = 08/16/14 Pct Recovery = 63% Analysis Date = 08/16/14 Pct Recovery = 63% Analysis Date = 08/11/14 Pct Recovery = 63% Analysis Date = 08/11/14 Pct Recovery = 63% Analysis Date = 08/06/14 Pct Recovery = 63% Analysis Date = 08/06/14 Pct Recovery = 63% Analysis Date = 08/01/14 Pct Recovery = 64% Analysis Date = 08/01/14 Pct Recovery = 64% Analysis Date = 07/27/14 Pct Recovery = 64% Analysis Date = 07/27/14 Pct Recovery = 64% Analysis Date = 07/22/14 Pct Recovery = 64% Analysis Date = 07/22/14 Pct Recovery = 64% Analysis Date = 07/17/14 Pct Recovery = 64% Analysis Date = 07/17/14 Pct Recovery = 64% Analysis Date = 07/12/14 Pct Recovery = 64% Analysis Date = 07/12/14 Pct Recovery = 64% Analysis Date = 07/07/14 Pct Recovery = 64% Analysis Date = 07/07/14 Pct Recovery = 64% Analysis Date = 07/02/14 Pct Recovery = 64% Analysis Date = 07/02/14 Pct Recovery = 64% Analysis Date = 06/27/14 Pct Recovery = 64% Analysis Date = 06/27/14 Pct Recovery = 64% Analysis Date = 06/22/14 Pct Recovery = 65% Analysis Date = 06/22/14 Pct Recovery = 65% Analysis Date = 06/17/14 Pct Recovery = 65% Analysis Date = 06/17/14 Pct Recovery = 65% Analysis Date = 06/12/14 Pct Recovery = 65% Analysis Date = 06/12/14 Pct Recovery = 65% Analysis Date = 06/07/14 Pct Recovery = 65% Analysis Date = 06/07/14 Pct Recovery = 65% Analysis Date = 06/02/14 Pct Recovery = 65% Analysis Date = 06/02/14 Pct Recovery = 65% Analysis Date = 05/28/14 Pct Recovery = 65% Analysis Date = 05/28/14 Pct Recovery = 65% Analysis Date = 05/23/14 Pct Recovery = 65% Analysis Date = 05/23/14 Pct Recovery = 65% Analysis Date = 05/18/14 Pct Recovery = 65% Analysis Date = 05/18/14 Pct Recovery = 65% Analysis Date = 05/13/14 Pct Recovery = 66% Analysis Date = 05/13/14 Pct Recovery = 66% Analysis Date = 05/08/14 Pct Recovery = 66% Analysis Date = 05/08/14 Pct Recovery = 66% Analysis Date = 05/03/14 Pct Recovery = 66% Analysis Date = 05/03/14 Pct Recovery = 66% Analysis Date = 04/28/14 Pct Recovery = 66% Analysis Date = 04/28/14 Pct Recovery = 66% Analysis Date = 04/23/14 Pct Recovery = 66% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
FEXOFENADINE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 7 71% 16% 71% 17%
>= Reporting Level 65 61% 9% 61% 8%
Total 72 62% 10% 61% 8%

Sample Statistics
FEXOFENADINE

Characteristic N % % Basis
Plotted 72 95% Spiked
Estimated Values 17 22% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 1 1% Spiked
Spiked 76 .  
False Negatives 3 4% 3 out of 76
Not Spiked 39 .  
False Positives 0 0% 0 out of 39

BQS OBSP Determination:
FLUCONAZOLE
METHOD: 2440 , TESTIDCODE: 67478LCM56
Open Data Set

Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 91% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 101% Analysis Date = 01/17/16 SpikeMix = ERA 0406-15-09: 80 µl & ERA 0406-15-07A: 80 µl Pct Recovery = 75% Analysis Date = 11/24/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 76% Analysis Date = 10/01/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 42% Analysis Date = 11/05/15 SpikeMix = ERA 0406-15-08: 80 µl & Abs 052215: 80 µl Pct Recovery = 73% Analysis Date = 11/04/15 SpikeMix = Abs 052215: 80 µl & Abs 050115: 80 µl Pct Recovery = 84% Analysis Date = 11/18/16 SpikeMix = ERA 04281604: 80 µl & ERA 04281603: 80 µl Pct Recovery = 81% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & ERA 04281604: 80 µl Pct Recovery = 79% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 71% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 71% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 82% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 88% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 79% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 77% Analysis Date = 05/07/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 100% Analysis Date = 04/29/15 SpikeMix = ERA 0319-14-05: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 114% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 104% Analysis Date = 01/16/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 108% Analysis Date = 12/07/14 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 115% Analysis Date = 12/06/14 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 87% Analysis Date = 08/28/14 SpikeMix = ERA 0319-14-04: 60 µl & ERA 0319-14-05: 60 µl Pct Recovery = 94% Analysis Date = 07/26/14 SpikeMix = ERA 0319-14-05: 60 µl & ERA 0318-14-02: 60 µl Pct Recovery = 104% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-04: 15 µl & Abs 041814: 15 µl Pct Recovery = 93% Analysis Date = 02/06/15 SpikeMix = Abs 041814: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 100% Analysis Date = 07/12/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 85% Analysis Date = 06/22/14 SpikeMix = Abs 041814: 60 µl & Abs 041614: 60 µl Pct Recovery = 107% Analysis Date = 05/21/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 77% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-08: 40 µl & ERA 0406-15-09: 40 µl Pct Recovery = 67% Analysis Date = 07/31/15 SpikeMix = ERA 0406-15-09: 40 µl & Abs 050115: 40 µl Pct Recovery = 89% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-08: 40 µl & Abs 052215: 40 µl Pct Recovery = 68% Analysis Date = 02/23/16 SpikeMix = Abs 052215: 40 µl & Abs 050115: 40 µl Pct Recovery = 92% Analysis Date = 09/10/15 SpikeMix = Abs 052215: 40 µl & ERA 0406-15-07A: 40 µl Pct Recovery = 61% Analysis Date = 07/31/15 SpikeMix = Abs 051315: 40 µl & Abs 052215: 40 µl Pct Recovery = 75% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 66% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 73% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 66% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 69% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 111% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 110% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 91% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 89% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 95% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 89% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 77% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 82% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 52% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 47% Analysis Date = 11/04/14 SpikeMix = Abs 041714: 8 µl & ERA 0319-14-05: 8 µl Pct Recovery = 82% Analysis Date = 10/24/14 SpikeMix = ERA 0319-14-05: 8 µl & Abs 041614: 8 µl Pct Recovery = 102% Analysis Date = 04/10/15 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 91% Analysis Date = 11/04/14 SpikeMix = Abs 041814: 8 µl & ERA 0318-14-02: 8 µl Pct Recovery = 95% Analysis Date = 10/11/14 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 86% Analysis Date = 08/30/14 SpikeMix = ERA 0318-14-02: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 94% Analysis Date = 08/16/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 51% Analysis Date = 07/13/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 79% Analysis Date = 10/10/14 SpikeMix = Abs 041714: 30 µl & Abs 041814: 30 µl Pct Recovery = 95% Analysis Date = 10/10/14 SpikeMix = Abs 041814: 30 µl & ERA 0318-14-02: 30 µl Pct Recovery = 98% Analysis Date = 07/13/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 71% Analysis Date = 05/30/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 93% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 71% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 90% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-08: 20 µl & ERA 0406-15-09: 20 µl Pct Recovery = 63% Analysis Date = 11/24/15 SpikeMix = ERA 0406-15-09: 20 µl & Abs 050115: 20 µl Pct Recovery = 74% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 76% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 73% Analysis Date = 02/23/16 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 71% Analysis Date = 11/24/15 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 76% Analysis Date = 09/09/15 SpikeMix = ERA 0406-15-08: 20 µl & Abs 052215: 20 µl Pct Recovery = 96% Analysis Date = 08/27/15 SpikeMix = Abs 052215: 20 µl & Abs 050115: 20 µl Pct Recovery = 84% Analysis Date = 07/09/15 SpikeMix = Abs 050115: 20 µl & Abs 052215: 20 µl Pct Recovery = 80% Analysis Date = 06/26/15 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 84% Analysis Date = 04/09/16 SpikeMix = Abs 051315: 10 µl & ERA 0406-15-09: 10 µl Pct Recovery = 71% Analysis Date = 04/09/16 SpikeMix = Abs 051315: 10 µl & ERA 0406-15-09: 10 µl Pct Recovery = 90% Analysis Date = 01/18/17 Pct Recovery = 88% Analysis Date = 01/14/17 Pct Recovery = 88% Analysis Date = 01/14/17 Pct Recovery = 88% Analysis Date = 01/09/17 Pct Recovery = 87% Analysis Date = 01/09/17 Pct Recovery = 87% Analysis Date = 01/04/17 Pct Recovery = 87% Analysis Date = 01/04/17 Pct Recovery = 87% Analysis Date = 12/30/16 Pct Recovery = 87% Analysis Date = 12/30/16 Pct Recovery = 87% Analysis Date = 12/25/16 Pct Recovery = 86% Analysis Date = 12/25/16 Pct Recovery = 86% Analysis Date = 12/20/16 Pct Recovery = 86% Analysis Date = 12/20/16 Pct Recovery = 86% Analysis Date = 12/15/16 Pct Recovery = 86% Analysis Date = 12/15/16 Pct Recovery = 86% Analysis Date = 12/11/16 Pct Recovery = 86% Analysis Date = 12/11/16 Pct Recovery = 86% Analysis Date = 12/06/16 Pct Recovery = 85% Analysis Date = 12/06/16 Pct Recovery = 85% Analysis Date = 12/01/16 Pct Recovery = 85% Analysis Date = 12/01/16 Pct Recovery = 85% Analysis Date = 11/26/16 Pct Recovery = 85% Analysis Date = 11/26/16 Pct Recovery = 85% Analysis Date = 11/21/16 Pct Recovery = 84% Analysis Date = 11/21/16 Pct Recovery = 84% Analysis Date = 11/16/16 Pct Recovery = 84% Analysis Date = 11/16/16 Pct Recovery = 84% Analysis Date = 11/11/16 Pct Recovery = 84% Analysis Date = 11/11/16 Pct Recovery = 84% Analysis Date = 11/06/16 Pct Recovery = 84% Analysis Date = 11/06/16 Pct Recovery = 84% Analysis Date = 11/02/16 Pct Recovery = 83% Analysis Date = 11/02/16 Pct Recovery = 83% Analysis Date = 10/28/16 Pct Recovery = 83% Analysis Date = 10/28/16 Pct Recovery = 83% Analysis Date = 10/23/16 Pct Recovery = 83% Analysis Date = 10/23/16 Pct Recovery = 83% Analysis Date = 10/18/16 Pct Recovery = 82% Analysis Date = 10/18/16 Pct Recovery = 82% Analysis Date = 10/13/16 Pct Recovery = 82% Analysis Date = 10/13/16 Pct Recovery = 82% Analysis Date = 10/08/16 Pct Recovery = 82% Analysis Date = 10/08/16 Pct Recovery = 82% Analysis Date = 10/03/16 Pct Recovery = 82% Analysis Date = 10/03/16 Pct Recovery = 82% Analysis Date = 09/28/16 Pct Recovery = 81% Analysis Date = 09/28/16 Pct Recovery = 81% Analysis Date = 09/24/16 Pct Recovery = 81% Analysis Date = 09/24/16 Pct Recovery = 81% Analysis Date = 09/19/16 Pct Recovery = 81% Analysis Date = 09/19/16 Pct Recovery = 81% Analysis Date = 09/14/16 Pct Recovery = 81% Analysis Date = 09/14/16 Pct Recovery = 81% Analysis Date = 09/09/16 Pct Recovery = 80% Analysis Date = 09/09/16 Pct Recovery = 80% Analysis Date = 09/04/16 Pct Recovery = 80% Analysis Date = 09/04/16 Pct Recovery = 80% Analysis Date = 08/30/16 Pct Recovery = 80% Analysis Date = 08/30/16 Pct Recovery = 80% Analysis Date = 08/25/16 Pct Recovery = 80% Analysis Date = 08/25/16 Pct Recovery = 80% Analysis Date = 08/21/16 Pct Recovery = 79% Analysis Date = 08/21/16 Pct Recovery = 79% Analysis Date = 08/16/16 Pct Recovery = 79% Analysis Date = 08/16/16 Pct Recovery = 79% Analysis Date = 08/11/16 Pct Recovery = 79% Analysis Date = 08/11/16 Pct Recovery = 79% Analysis Date = 08/06/16 Pct Recovery = 79% Analysis Date = 08/06/16 Pct Recovery = 79% Analysis Date = 08/01/16 Pct Recovery = 79% Analysis Date = 08/01/16 Pct Recovery = 79% Analysis Date = 07/27/16 Pct Recovery = 78% Analysis Date = 07/27/16 Pct Recovery = 78% Analysis Date = 07/22/16 Pct Recovery = 78% Analysis Date = 07/22/16 Pct Recovery = 78% Analysis Date = 07/17/16 Pct Recovery = 78% Analysis Date = 07/17/16 Pct Recovery = 78% Analysis Date = 07/13/16 Pct Recovery = 78% Analysis Date = 07/13/16 Pct Recovery = 78% Analysis Date = 07/08/16 Pct Recovery = 78% Analysis Date = 07/08/16 Pct Recovery = 78% Analysis Date = 07/03/16 Pct Recovery = 78% Analysis Date = 07/03/16 Pct Recovery = 78% Analysis Date = 06/28/16 Pct Recovery = 77% Analysis Date = 06/28/16 Pct Recovery = 77% Analysis Date = 06/23/16 Pct Recovery = 77% Analysis Date = 06/23/16 Pct Recovery = 77% Analysis Date = 06/18/16 Pct Recovery = 77% Analysis Date = 06/18/16 Pct Recovery = 77% Analysis Date = 06/13/16 Pct Recovery = 77% Analysis Date = 06/13/16 Pct Recovery = 77% Analysis Date = 06/08/16 Pct Recovery = 77% Analysis Date = 06/08/16 Pct Recovery = 77% Analysis Date = 06/04/16 Pct Recovery = 77% Analysis Date = 06/04/16 Pct Recovery = 77% Analysis Date = 05/30/16 Pct Recovery = 77% Analysis Date = 05/30/16 Pct Recovery = 77% Analysis Date = 05/25/16 Pct Recovery = 77% Analysis Date = 05/25/16 Pct Recovery = 77% Analysis Date = 05/20/16 Pct Recovery = 76% Analysis Date = 05/20/16 Pct Recovery = 76% Analysis Date = 05/15/16 Pct Recovery = 76% Analysis Date = 05/15/16 Pct Recovery = 76% Analysis Date = 05/10/16 Pct Recovery = 76% Analysis Date = 05/10/16 Pct Recovery = 76% Analysis Date = 05/05/16 Pct Recovery = 76% Analysis Date = 05/05/16 Pct Recovery = 76% Analysis Date = 05/01/16 Pct Recovery = 76% Analysis Date = 05/01/16 Pct Recovery = 76% Analysis Date = 04/26/16 Pct Recovery = 76% Analysis Date = 04/26/16 Pct Recovery = 76% Analysis Date = 04/21/16 Pct Recovery = 76% Analysis Date = 04/21/16 Pct Recovery = 76% Analysis Date = 04/16/16 Pct Recovery = 76% Analysis Date = 04/16/16 Pct Recovery = 76% Analysis Date = 04/11/16 Pct Recovery = 75% Analysis Date = 04/11/16 Pct Recovery = 75% Analysis Date = 04/06/16 Pct Recovery = 75% Analysis Date = 04/06/16 Pct Recovery = 75% Analysis Date = 04/01/16 Pct Recovery = 75% Analysis Date = 04/01/16 Pct Recovery = 75% Analysis Date = 03/27/16 Pct Recovery = 75% Analysis Date = 03/27/16 Pct Recovery = 75% Analysis Date = 03/23/16 Pct Recovery = 75% Analysis Date = 03/23/16 Pct Recovery = 75% Analysis Date = 03/18/16 Pct Recovery = 75% Analysis Date = 03/18/16 Pct Recovery = 75% Analysis Date = 03/13/16 Pct Recovery = 75% Analysis Date = 03/13/16 Pct Recovery = 75% Analysis Date = 03/08/16 Pct Recovery = 75% Analysis Date = 03/08/16 Pct Recovery = 75% Analysis Date = 03/03/16 Pct Recovery = 75% Analysis Date = 03/03/16 Pct Recovery = 75% Analysis Date = 02/27/16 Pct Recovery = 75% Analysis Date = 02/27/16 Pct Recovery = 75% Analysis Date = 02/22/16 Pct Recovery = 75% Analysis Date = 02/22/16 Pct Recovery = 75% Analysis Date = 02/17/16 Pct Recovery = 75% Analysis Date = 02/17/16 Pct Recovery = 75% Analysis Date = 02/13/16 Pct Recovery = 75% Analysis Date = 02/13/16 Pct Recovery = 75% Analysis Date = 02/08/16 Pct Recovery = 75% Analysis Date = 02/08/16 Pct Recovery = 75% Analysis Date = 02/03/16 Pct Recovery = 75% Analysis Date = 02/03/16 Pct Recovery = 75% Analysis Date = 01/29/16 Pct Recovery = 75% Analysis Date = 01/29/16 Pct Recovery = 75% Analysis Date = 01/24/16 Pct Recovery = 76% Analysis Date = 01/24/16 Pct Recovery = 76% Analysis Date = 01/19/16 Pct Recovery = 76% Analysis Date = 01/19/16 Pct Recovery = 76% Analysis Date = 01/14/16 Pct Recovery = 76% Analysis Date = 01/14/16 Pct Recovery = 76% Analysis Date = 01/10/16 Pct Recovery = 76% Analysis Date = 01/10/16 Pct Recovery = 76% Analysis Date = 01/05/16 Pct Recovery = 76% Analysis Date = 01/05/16 Pct Recovery = 76% Analysis Date = 12/31/15 Pct Recovery = 76% Analysis Date = 12/31/15 Pct Recovery = 76% Analysis Date = 12/26/15 Pct Recovery = 76% Analysis Date = 12/26/15 Pct Recovery = 76% Analysis Date = 12/21/15 Pct Recovery = 76% Analysis Date = 12/21/15 Pct Recovery = 76% Analysis Date = 12/16/15 Pct Recovery = 76% Analysis Date = 12/16/15 Pct Recovery = 76% Analysis Date = 12/11/15 Pct Recovery = 77% Analysis Date = 12/11/15 Pct Recovery = 77% Analysis Date = 12/06/15 Pct Recovery = 77% Analysis Date = 12/06/15 Pct Recovery = 77% Analysis Date = 12/02/15 Pct Recovery = 77% Analysis Date = 12/02/15 Pct Recovery = 77% Analysis Date = 11/27/15 Pct Recovery = 77% Analysis Date = 11/27/15 Pct Recovery = 77% Analysis Date = 11/22/15 Pct Recovery = 77% Analysis Date = 11/22/15 Pct Recovery = 77% Analysis Date = 11/17/15 Pct Recovery = 77% Analysis Date = 11/17/15 Pct Recovery = 77% Analysis Date = 11/12/15 Pct Recovery = 78% Analysis Date = 11/12/15 Pct Recovery = 78% Analysis Date = 11/07/15 Pct Recovery = 78% Analysis Date = 11/07/15 Pct Recovery = 78% Analysis Date = 11/02/15 Pct Recovery = 78% Analysis Date = 11/02/15 Pct Recovery = 78% Analysis Date = 10/28/15 Pct Recovery = 79% Analysis Date = 10/28/15 Pct Recovery = 79% Analysis Date = 10/24/15 Pct Recovery = 79% Analysis Date = 10/24/15 Pct Recovery = 79% Analysis Date = 10/19/15 Pct Recovery = 79% Analysis Date = 10/19/15 Pct Recovery = 79% Analysis Date = 10/14/15 Pct Recovery = 80% Analysis Date = 10/14/15 Pct Recovery = 80% Analysis Date = 10/09/15 Pct Recovery = 80% Analysis Date = 10/09/15 Pct Recovery = 80% Analysis Date = 10/04/15 Pct Recovery = 80% Analysis Date = 10/04/15 Pct Recovery = 80% Analysis Date = 09/29/15 Pct Recovery = 80% Analysis Date = 09/29/15 Pct Recovery = 80% Analysis Date = 09/24/15 Pct Recovery = 81% Analysis Date = 09/24/15 Pct Recovery = 81% Analysis Date = 09/19/15 Pct Recovery = 81% Analysis Date = 09/19/15 Pct Recovery = 81% Analysis Date = 09/15/15 Pct Recovery = 81% Analysis Date = 09/15/15 Pct Recovery = 81% Analysis Date = 09/10/15 Pct Recovery = 82% Analysis Date = 09/10/15 Pct Recovery = 82% Analysis Date = 09/05/15 Pct Recovery = 82% Analysis Date = 09/05/15 Pct Recovery = 82% Analysis Date = 08/31/15 Pct Recovery = 82% Analysis Date = 08/31/15 Pct Recovery = 82% Analysis Date = 08/26/15 Pct Recovery = 82% Analysis Date = 08/26/15 Pct Recovery = 82% Analysis Date = 08/21/15 Pct Recovery = 83% Analysis Date = 08/21/15 Pct Recovery = 83% Analysis Date = 08/16/15 Pct Recovery = 83% Analysis Date = 08/16/15 Pct Recovery = 83% Analysis Date = 08/12/15 Pct Recovery = 83% Analysis Date = 08/12/15 Pct Recovery = 83% Analysis Date = 08/07/15 Pct Recovery = 84% Analysis Date = 08/07/15 Pct Recovery = 84% Analysis Date = 08/02/15 Pct Recovery = 84% Analysis Date = 08/02/15 Pct Recovery = 84% Analysis Date = 07/28/15 Pct Recovery = 84% Analysis Date = 07/28/15 Pct Recovery = 84% Analysis Date = 07/23/15 Pct Recovery = 84% Analysis Date = 07/23/15 Pct Recovery = 84% Analysis Date = 07/18/15 Pct Recovery = 85% Analysis Date = 07/18/15 Pct Recovery = 85% Analysis Date = 07/13/15 Pct Recovery = 85% Analysis Date = 07/13/15 Pct Recovery = 85% Analysis Date = 07/08/15 Pct Recovery = 85% Analysis Date = 07/08/15 Pct Recovery = 85% Analysis Date = 07/04/15 Pct Recovery = 85% Analysis Date = 07/04/15 Pct Recovery = 85% Analysis Date = 06/29/15 Pct Recovery = 86% Analysis Date = 06/29/15 Pct Recovery = 86% Analysis Date = 06/24/15 Pct Recovery = 86% Analysis Date = 06/24/15 Pct Recovery = 86% Analysis Date = 06/19/15 Pct Recovery = 86% Analysis Date = 06/19/15 Pct Recovery = 86% Analysis Date = 06/14/15 Pct Recovery = 86% Analysis Date = 06/14/15 Pct Recovery = 86% Analysis Date = 06/09/15 Pct Recovery = 86% Analysis Date = 06/09/15 Pct Recovery = 86% Analysis Date = 06/04/15 Pct Recovery = 87% Analysis Date = 06/04/15 Pct Recovery = 87% Analysis Date = 05/30/15 Pct Recovery = 87% Analysis Date = 05/30/15 Pct Recovery = 87% Analysis Date = 05/26/15 Pct Recovery = 87% Analysis Date = 05/26/15 Pct Recovery = 87% Analysis Date = 05/21/15 Pct Recovery = 87% Analysis Date = 05/21/15 Pct Recovery = 87% Analysis Date = 05/16/15 Pct Recovery = 87% Analysis Date = 05/16/15 Pct Recovery = 87% Analysis Date = 05/11/15 Pct Recovery = 88% Analysis Date = 05/11/15 Pct Recovery = 88% Analysis Date = 05/06/15 Pct Recovery = 88% Analysis Date = 05/06/15 Pct Recovery = 88% Analysis Date = 05/01/15 Pct Recovery = 88% Analysis Date = 05/01/15 Pct Recovery = 88% Analysis Date = 04/26/15 Pct Recovery = 88% Analysis Date = 04/26/15 Pct Recovery = 88% Analysis Date = 04/22/15 Pct Recovery = 88% Analysis Date = 04/22/15 Pct Recovery = 88% Analysis Date = 04/17/15 Pct Recovery = 88% Analysis Date = 04/17/15 Pct Recovery = 88% Analysis Date = 04/12/15 Pct Recovery = 89% Analysis Date = 04/12/15 Pct Recovery = 89% Analysis Date = 04/07/15 Pct Recovery = 89% Analysis Date = 04/07/15 Pct Recovery = 89% Analysis Date = 04/02/15 Pct Recovery = 89% Analysis Date = 04/02/15 Pct Recovery = 89% Analysis Date = 03/28/15 Pct Recovery = 89% Analysis Date = 03/28/15 Pct Recovery = 89% Analysis Date = 03/23/15 Pct Recovery = 89% Analysis Date = 03/23/15 Pct Recovery = 89% Analysis Date = 03/18/15 Pct Recovery = 89% Analysis Date = 03/18/15 Pct Recovery = 89% Analysis Date = 03/14/15 Pct Recovery = 89% Analysis Date = 03/14/15 Pct Recovery = 89% Analysis Date = 03/09/15 Pct Recovery = 89% Analysis Date = 03/09/15 Pct Recovery = 89% Analysis Date = 03/04/15 Pct Recovery = 89% Analysis Date = 03/04/15 Pct Recovery = 89% Analysis Date = 02/27/15 Pct Recovery = 89% Analysis Date = 02/27/15 Pct Recovery = 89% Analysis Date = 02/22/15 Pct Recovery = 89% Analysis Date = 02/22/15 Pct Recovery = 89% Analysis Date = 02/17/15 Pct Recovery = 89% Analysis Date = 02/17/15 Pct Recovery = 89% Analysis Date = 02/12/15 Pct Recovery = 89% Analysis Date = 02/12/15 Pct Recovery = 89% Analysis Date = 02/07/15 Pct Recovery = 90% Analysis Date = 02/07/15 Pct Recovery = 90% Analysis Date = 02/03/15 Pct Recovery = 90% Analysis Date = 02/03/15 Pct Recovery = 90% Analysis Date = 01/29/15 Pct Recovery = 90% Analysis Date = 01/29/15 Pct Recovery = 90% Analysis Date = 01/24/15 Pct Recovery = 90% Analysis Date = 01/24/15 Pct Recovery = 90% Analysis Date = 01/19/15 Pct Recovery = 90% Analysis Date = 01/19/15 Pct Recovery = 90% Analysis Date = 01/14/15 Pct Recovery = 90% Analysis Date = 01/14/15 Pct Recovery = 90% Analysis Date = 01/09/15 Pct Recovery = 90% Analysis Date = 01/09/15 Pct Recovery = 90% Analysis Date = 01/04/15 Pct Recovery = 90% Analysis Date = 01/04/15 Pct Recovery = 90% Analysis Date = 12/31/14 Pct Recovery = 90% Analysis Date = 12/31/14 Pct Recovery = 90% Analysis Date = 12/26/14 Pct Recovery = 90% Analysis Date = 12/26/14 Pct Recovery = 90% Analysis Date = 12/21/14 Pct Recovery = 90% Analysis Date = 12/21/14 Pct Recovery = 90% Analysis Date = 12/16/14 Pct Recovery = 90% Analysis Date = 12/16/14 Pct Recovery = 90% Analysis Date = 12/11/14 Pct Recovery = 90% Analysis Date = 12/11/14 Pct Recovery = 90% Analysis Date = 12/06/14 Pct Recovery = 90% Analysis Date = 12/06/14 Pct Recovery = 90% Analysis Date = 12/01/14 Pct Recovery = 90% Analysis Date = 12/01/14 Pct Recovery = 90% Analysis Date = 11/26/14 Pct Recovery = 90% Analysis Date = 11/26/14 Pct Recovery = 90% Analysis Date = 11/22/14 Pct Recovery = 90% Analysis Date = 11/22/14 Pct Recovery = 90% Analysis Date = 11/17/14 Pct Recovery = 91% Analysis Date = 11/17/14 Pct Recovery = 91% Analysis Date = 11/12/14 Pct Recovery = 91% Analysis Date = 11/12/14 Pct Recovery = 91% Analysis Date = 11/07/14 Pct Recovery = 91% Analysis Date = 11/07/14 Pct Recovery = 91% Analysis Date = 11/02/14 Pct Recovery = 91% Analysis Date = 11/02/14 Pct Recovery = 91% Analysis Date = 10/28/14 Pct Recovery = 91% Analysis Date = 10/28/14 Pct Recovery = 91% Analysis Date = 10/23/14 Pct Recovery = 91% Analysis Date = 10/23/14 Pct Recovery = 91% Analysis Date = 10/18/14 Pct Recovery = 91% Analysis Date = 10/18/14 Pct Recovery = 91% Analysis Date = 10/14/14 Pct Recovery = 91% Analysis Date = 10/14/14 Pct Recovery = 91% Analysis Date = 10/09/14 Pct Recovery = 91% Analysis Date = 10/09/14 Pct Recovery = 91% Analysis Date = 10/04/14 Pct Recovery = 91% Analysis Date = 10/04/14 Pct Recovery = 91% Analysis Date = 09/29/14 Pct Recovery = 91% Analysis Date = 09/29/14 Pct Recovery = 91% Analysis Date = 09/24/14 Pct Recovery = 91% Analysis Date = 09/24/14 Pct Recovery = 91% Analysis Date = 09/19/14 Pct Recovery = 91% Analysis Date = 09/19/14 Pct Recovery = 91% Analysis Date = 09/14/14 Pct Recovery = 91% Analysis Date = 09/14/14 Pct Recovery = 91% Analysis Date = 09/10/14 Pct Recovery = 91% Analysis Date = 09/10/14 Pct Recovery = 91% Analysis Date = 09/05/14 Pct Recovery = 91% Analysis Date = 09/05/14 Pct Recovery = 91% Analysis Date = 08/31/14 Pct Recovery = 91% Analysis Date = 08/31/14 Pct Recovery = 91% Analysis Date = 08/26/14 Pct Recovery = 91% Analysis Date = 08/26/14 Pct Recovery = 91% Analysis Date = 08/21/14 Pct Recovery = 91% Analysis Date = 08/21/14 Pct Recovery = 91% Analysis Date = 08/16/14 Pct Recovery = 91% Analysis Date = 08/16/14 Pct Recovery = 91% Analysis Date = 08/11/14 Pct Recovery = 91% Analysis Date = 08/11/14 Pct Recovery = 91% Analysis Date = 08/06/14 Pct Recovery = 91% Analysis Date = 08/06/14 Pct Recovery = 91% Analysis Date = 08/02/14 Pct Recovery = 91% Analysis Date = 08/02/14 Pct Recovery = 91% Analysis Date = 07/28/14 Pct Recovery = 91% Analysis Date = 07/28/14 Pct Recovery = 91% Analysis Date = 07/23/14 Pct Recovery = 91% Analysis Date = 07/23/14 Pct Recovery = 91% Analysis Date = 07/18/14 Pct Recovery = 91% Analysis Date = 07/18/14 Pct Recovery = 91% Analysis Date = 07/13/14 Pct Recovery = 91% Analysis Date = 07/13/14 Pct Recovery = 91% Analysis Date = 07/08/14 Pct Recovery = 91% Analysis Date = 07/08/14 Pct Recovery = 91% Analysis Date = 07/03/14 Pct Recovery = 91% Analysis Date = 07/03/14 Pct Recovery = 91% Analysis Date = 06/28/14 Pct Recovery = 91% Analysis Date = 06/28/14 Pct Recovery = 91% Analysis Date = 06/24/14 Pct Recovery = 91% Analysis Date = 06/24/14 Pct Recovery = 91% Analysis Date = 06/19/14 Pct Recovery = 91% Analysis Date = 06/19/14 Pct Recovery = 91% Analysis Date = 06/14/14 Pct Recovery = 91% Analysis Date = 06/14/14 Pct Recovery = 91% Analysis Date = 06/09/14 Pct Recovery = 91% Analysis Date = 06/09/14 Pct Recovery = 91% Analysis Date = 06/04/14 Pct Recovery = 91% Analysis Date = 06/04/14 Pct Recovery = 91% Analysis Date = 05/30/14 Pct Recovery = 90% Analysis Date = 05/30/14 Pct Recovery = 90% Analysis Date = 05/25/14 Pct Recovery = 90% Analysis Date = 05/25/14 Pct Recovery = 90% Analysis Date = 05/21/14 Pct Recovery = 90% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
FLUCONAZOLE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 2 80% 13% 80% 14%
>= Reporting Level 72 83% 16% 83% 15%
Total 74 83% 16% 83% 15%

Sample Statistics
FLUCONAZOLE

Characteristic N % % Basis
Plotted 74 99% Spiked
Estimated Values 6 8% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 75 .  
False Negatives 1 1% 1 out of 75
Not Spiked 40 .  
False Positives 0 0% 0 out of 40

BQS OBSP Determination:
FLUOXETINE
METHOD: 2440 , TESTIDCODE: 67450LCM56
Open Data Set

Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 66% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 74% Analysis Date = 01/17/16 SpikeMix = ERA 0406-15-09: 80 µl & ERA 0406-15-07A: 80 µl Pct Recovery = 63% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 80 µl & Abs 051315: 80 µl Pct Recovery = 53% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 80 µl & ERA 0406-15-08: 80 µl Pct Recovery = 56% Analysis Date = 11/04/15 SpikeMix = Abs 052215: 80 µl & Abs 050115: 80 µl Pct Recovery = 58% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 66% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 73% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 73% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 65% Analysis Date = 11/18/16 SpikeMix = ERA 04281604: 80 µl & ERA 04281603: 80 µl Pct Recovery = 59% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & ERA 04281604: 80 µl Pct Recovery = 63% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 55% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 51% Analysis Date = 05/07/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 75% Analysis Date = 04/29/15 SpikeMix = ERA 0319-14-05: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 77% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 54% Analysis Date = 01/16/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 54% Analysis Date = 12/07/14 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 61% Analysis Date = 12/06/14 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 48% Analysis Date = 08/28/14 SpikeMix = ERA 0319-14-04: 60 µl & ERA 0319-14-05: 60 µl Pct Recovery = 48% Analysis Date = 07/26/14 SpikeMix = ERA 0319-14-05: 60 µl & ERA 0318-14-02: 60 µl Pct Recovery = 71% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-04: 15 µl & Abs 041814: 15 µl Pct Recovery = 52% Analysis Date = 02/06/15 SpikeMix = Abs 041814: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 52% Analysis Date = 07/12/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 57% Analysis Date = 06/22/14 SpikeMix = Abs 041814: 60 µl & Abs 041614: 60 µl Pct Recovery = 71% Analysis Date = 05/21/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 71% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-07A: 40 µl & Abs 051315: 40 µl Pct Recovery = 51% Analysis Date = 11/04/15 SpikeMix = ERA 0406-15-07A: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 57% Analysis Date = 09/10/15 SpikeMix = Abs 052215: 40 µl & ERA 0406-15-07A: 40 µl Pct Recovery = 61% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 53% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 52% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 44% Analysis Date = 02/23/16 SpikeMix = Abs 052215: 40 µl & Abs 050115: 40 µl Pct Recovery = 61% Analysis Date = 07/31/15 SpikeMix = ERA 0406-15-09: 40 µl & Abs 050115: 40 µl Pct Recovery = 88% Analysis Date = 07/30/15 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 78% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 78% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 143% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 73% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 72% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 57% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 65% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 43% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 54% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 51% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 49% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 55% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 63% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 38% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 50% Analysis Date = 11/04/14 SpikeMix = Abs 041714: 8 µl & ERA 0319-14-05: 8 µl Pct Recovery = 41% Analysis Date = 10/24/14 SpikeMix = ERA 0319-14-05: 8 µl & Abs 041614: 8 µl Pct Recovery = 47% Analysis Date = 11/04/14 SpikeMix = Abs 041814: 8 µl & ERA 0318-14-02: 8 µl Pct Recovery = 44% Analysis Date = 10/11/14 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 51% Analysis Date = 04/23/14 SpikeMix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.2: 20 µl Pct Recovery = 58% Analysis Date = 08/30/14 SpikeMix = ERA 0318-14-02: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 61% Analysis Date = 10/10/14 SpikeMix = Abs 041714: 30 µl & Abs 041814: 30 µl Pct Recovery = 63% Analysis Date = 10/10/14 SpikeMix = Abs 041814: 30 µl & ERA 0318-14-02: 30 µl Pct Recovery = 51% Analysis Date = 07/13/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 45% Analysis Date = 05/30/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 73% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 56% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 56% Analysis Date = 04/27/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 76% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 60% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 57% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 46% Analysis Date = 11/24/15 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 54% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-09: 20 µl Pct Recovery = 42% Analysis Date = 09/15/15 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 66% Analysis Date = 11/25/15 SpikeMix = Abs 050115: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 52% Analysis Date = 11/24/15 SpikeMix = ERA 0406-15-09: 20 µl & Abs 050115: 20 µl Pct Recovery = 60% Analysis Date = 08/27/15 SpikeMix = Abs 052215: 20 µl & Abs 050115: 20 µl Pct Recovery = 50% Analysis Date = 08/11/15 SpikeMix = Abs 050115: 20 µl & Abs 051315: 20 µl Pct Recovery = 52% Analysis Date = 07/09/15 SpikeMix = Abs 050115: 20 µl & Abs 052215: 20 µl Pct Recovery = 44% Analysis Date = 06/09/15 SpikeMix = Abs 051315: 20 µl & Abs 050115: 20 µl Pct Recovery = 58% Analysis Date = 01/18/17 Pct Recovery = 72% Analysis Date = 01/13/17 Pct Recovery = 72% Analysis Date = 01/13/17 Pct Recovery = 72% Analysis Date = 01/08/17 Pct Recovery = 72% Analysis Date = 01/08/17 Pct Recovery = 72% Analysis Date = 01/03/17 Pct Recovery = 71% Analysis Date = 01/03/17 Pct Recovery = 71% Analysis Date = 12/29/16 Pct Recovery = 71% Analysis Date = 12/29/16 Pct Recovery = 71% Analysis Date = 12/24/16 Pct Recovery = 71% Analysis Date = 12/24/16 Pct Recovery = 71% Analysis Date = 12/19/16 Pct Recovery = 70% Analysis Date = 12/19/16 Pct Recovery = 70% Analysis Date = 12/14/16 Pct Recovery = 70% Analysis Date = 12/14/16 Pct Recovery = 70% Analysis Date = 12/09/16 Pct Recovery = 69% Analysis Date = 12/09/16 Pct Recovery = 69% Analysis Date = 12/04/16 Pct Recovery = 69% Analysis Date = 12/04/16 Pct Recovery = 69% Analysis Date = 11/29/16 Pct Recovery = 69% Analysis Date = 11/29/16 Pct Recovery = 69% Analysis Date = 11/24/16 Pct Recovery = 68% Analysis Date = 11/24/16 Pct Recovery = 68% Analysis Date = 11/19/16 Pct Recovery = 68% Analysis Date = 11/19/16 Pct Recovery = 68% Analysis Date = 11/14/16 Pct Recovery = 68% Analysis Date = 11/14/16 Pct Recovery = 68% Analysis Date = 11/09/16 Pct Recovery = 67% Analysis Date = 11/09/16 Pct Recovery = 67% Analysis Date = 11/04/16 Pct Recovery = 67% Analysis Date = 11/04/16 Pct Recovery = 67% Analysis Date = 10/30/16 Pct Recovery = 66% Analysis Date = 10/30/16 Pct Recovery = 66% Analysis Date = 10/25/16 Pct Recovery = 66% Analysis Date = 10/25/16 Pct Recovery = 66% Analysis Date = 10/20/16 Pct Recovery = 66% Analysis Date = 10/20/16 Pct Recovery = 66% Analysis Date = 10/15/16 Pct Recovery = 65% Analysis Date = 10/15/16 Pct Recovery = 65% Analysis Date = 10/10/16 Pct Recovery = 65% Analysis Date = 10/10/16 Pct Recovery = 65% Analysis Date = 10/05/16 Pct Recovery = 65% Analysis Date = 10/05/16 Pct Recovery = 65% Analysis Date = 09/30/16 Pct Recovery = 64% Analysis Date = 09/30/16 Pct Recovery = 64% Analysis Date = 09/25/16 Pct Recovery = 64% Analysis Date = 09/25/16 Pct Recovery = 64% Analysis Date = 09/20/16 Pct Recovery = 64% Analysis Date = 09/20/16 Pct Recovery = 64% Analysis Date = 09/15/16 Pct Recovery = 63% Analysis Date = 09/15/16 Pct Recovery = 63% Analysis Date = 09/10/16 Pct Recovery = 63% Analysis Date = 09/10/16 Pct Recovery = 63% Analysis Date = 09/05/16 Pct Recovery = 63% Analysis Date = 09/05/16 Pct Recovery = 63% Analysis Date = 08/31/16 Pct Recovery = 62% Analysis Date = 08/31/16 Pct Recovery = 62% Analysis Date = 08/26/16 Pct Recovery = 62% Analysis Date = 08/26/16 Pct Recovery = 62% Analysis Date = 08/21/16 Pct Recovery = 62% Analysis Date = 08/21/16 Pct Recovery = 62% Analysis Date = 08/16/16 Pct Recovery = 61% Analysis Date = 08/16/16 Pct Recovery = 61% Analysis Date = 08/11/16 Pct Recovery = 61% Analysis Date = 08/11/16 Pct Recovery = 61% Analysis Date = 08/06/16 Pct Recovery = 61% Analysis Date = 08/06/16 Pct Recovery = 61% Analysis Date = 08/01/16 Pct Recovery = 61% Analysis Date = 08/01/16 Pct Recovery = 61% Analysis Date = 07/27/16 Pct Recovery = 61% Analysis Date = 07/27/16 Pct Recovery = 61% Analysis Date = 07/22/16 Pct Recovery = 60% Analysis Date = 07/22/16 Pct Recovery = 60% Analysis Date = 07/17/16 Pct Recovery = 60% Analysis Date = 07/17/16 Pct Recovery = 60% Analysis Date = 07/12/16 Pct Recovery = 60% Analysis Date = 07/12/16 Pct Recovery = 60% Analysis Date = 07/07/16 Pct Recovery = 60% Analysis Date = 07/07/16 Pct Recovery = 60% Analysis Date = 07/02/16 Pct Recovery = 60% Analysis Date = 07/02/16 Pct Recovery = 60% Analysis Date = 06/27/16 Pct Recovery = 59% Analysis Date = 06/27/16 Pct Recovery = 59% Analysis Date = 06/22/16 Pct Recovery = 59% Analysis Date = 06/22/16 Pct Recovery = 59% Analysis Date = 06/17/16 Pct Recovery = 59% Analysis Date = 06/17/16 Pct Recovery = 59% Analysis Date = 06/12/16 Pct Recovery = 59% Analysis Date = 06/12/16 Pct Recovery = 59% Analysis Date = 06/07/16 Pct Recovery = 59% Analysis Date = 06/07/16 Pct Recovery = 59% Analysis Date = 06/02/16 Pct Recovery = 58% Analysis Date = 06/02/16 Pct Recovery = 58% Analysis Date = 05/28/16 Pct Recovery = 58% Analysis Date = 05/28/16 Pct Recovery = 58% Analysis Date = 05/23/16 Pct Recovery = 58% Analysis Date = 05/23/16 Pct Recovery = 58% Analysis Date = 05/18/16 Pct Recovery = 58% Analysis Date = 05/18/16 Pct Recovery = 58% Analysis Date = 05/13/16 Pct Recovery = 57% Analysis Date = 05/13/16 Pct Recovery = 57% Analysis Date = 05/08/16 Pct Recovery = 57% Analysis Date = 05/08/16 Pct Recovery = 57% Analysis Date = 05/03/16 Pct Recovery = 57% Analysis Date = 05/03/16 Pct Recovery = 57% Analysis Date = 04/28/16 Pct Recovery = 57% Analysis Date = 04/28/16 Pct Recovery = 57% Analysis Date = 04/23/16 Pct Recovery = 57% Analysis Date = 04/23/16 Pct Recovery = 57% Analysis Date = 04/18/16 Pct Recovery = 57% Analysis Date = 04/18/16 Pct Recovery = 57% Analysis Date = 04/13/16 Pct Recovery = 57% Analysis Date = 04/13/16 Pct Recovery = 57% Analysis Date = 04/08/16 Pct Recovery = 57% Analysis Date = 04/08/16 Pct Recovery = 57% Analysis Date = 04/03/16 Pct Recovery = 57% Analysis Date = 04/03/16 Pct Recovery = 57% Analysis Date = 03/29/16 Pct Recovery = 57% Analysis Date = 03/29/16 Pct Recovery = 57% Analysis Date = 03/24/16 Pct Recovery = 57% Analysis Date = 03/24/16 Pct Recovery = 57% Analysis Date = 03/19/16 Pct Recovery = 57% Analysis Date = 03/19/16 Pct Recovery = 57% Analysis Date = 03/14/16 Pct Recovery = 57% Analysis Date = 03/14/16 Pct Recovery = 57% Analysis Date = 03/09/16 Pct Recovery = 57% Analysis Date = 03/09/16 Pct Recovery = 57% Analysis Date = 03/04/16 Pct Recovery = 57% Analysis Date = 03/04/16 Pct Recovery = 57% Analysis Date = 02/28/16 Pct Recovery = 57% Analysis Date = 02/28/16 Pct Recovery = 57% Analysis Date = 02/23/16 Pct Recovery = 57% Analysis Date = 02/23/16 Pct Recovery = 57% Analysis Date = 02/18/16 Pct Recovery = 57% Analysis Date = 02/18/16 Pct Recovery = 57% Analysis Date = 02/13/16 Pct Recovery = 57% Analysis Date = 02/13/16 Pct Recovery = 57% Analysis Date = 02/08/16 Pct Recovery = 57% Analysis Date = 02/08/16 Pct Recovery = 57% Analysis Date = 02/03/16 Pct Recovery = 57% Analysis Date = 02/03/16 Pct Recovery = 57% Analysis Date = 01/29/16 Pct Recovery = 57% Analysis Date = 01/29/16 Pct Recovery = 57% Analysis Date = 01/24/16 Pct Recovery = 57% Analysis Date = 01/24/16 Pct Recovery = 57% Analysis Date = 01/19/16 Pct Recovery = 57% Analysis Date = 01/19/16 Pct Recovery = 57% Analysis Date = 01/14/16 Pct Recovery = 57% Analysis Date = 01/14/16 Pct Recovery = 57% Analysis Date = 01/09/16 Pct Recovery = 57% Analysis Date = 01/09/16 Pct Recovery = 57% Analysis Date = 01/04/16 Pct Recovery = 57% Analysis Date = 01/04/16 Pct Recovery = 57% Analysis Date = 12/30/15 Pct Recovery = 57% Analysis Date = 12/30/15 Pct Recovery = 57% Analysis Date = 12/25/15 Pct Recovery = 57% Analysis Date = 12/25/15 Pct Recovery = 57% Analysis Date = 12/20/15 Pct Recovery = 57% Analysis Date = 12/20/15 Pct Recovery = 57% Analysis Date = 12/15/15 Pct Recovery = 58% Analysis Date = 12/15/15 Pct Recovery = 58% Analysis Date = 12/10/15 Pct Recovery = 58% Analysis Date = 12/10/15 Pct Recovery = 58% Analysis Date = 12/05/15 Pct Recovery = 58% Analysis Date = 12/05/15 Pct Recovery = 58% Analysis Date = 11/30/15 Pct Recovery = 58% Analysis Date = 11/30/15 Pct Recovery = 58% Analysis Date = 11/25/15 Pct Recovery = 58% Analysis Date = 11/25/15 Pct Recovery = 58% Analysis Date = 11/20/15 Pct Recovery = 58% Analysis Date = 11/20/15 Pct Recovery = 58% Analysis Date = 11/15/15 Pct Recovery = 58% Analysis Date = 11/15/15 Pct Recovery = 58% Analysis Date = 11/10/15 Pct Recovery = 58% Analysis Date = 11/10/15 Pct Recovery = 58% Analysis Date = 11/05/15 Pct Recovery = 58% Analysis Date = 11/05/15 Pct Recovery = 58% Analysis Date = 10/31/15 Pct Recovery = 58% Analysis Date = 10/31/15 Pct Recovery = 58% Analysis Date = 10/26/15 Pct Recovery = 58% Analysis Date = 10/26/15 Pct Recovery = 58% Analysis Date = 10/21/15 Pct Recovery = 58% Analysis Date = 10/21/15 Pct Recovery = 58% Analysis Date = 10/16/15 Pct Recovery = 58% Analysis Date = 10/16/15 Pct Recovery = 58% Analysis Date = 10/11/15 Pct Recovery = 58% Analysis Date = 10/11/15 Pct Recovery = 58% Analysis Date = 10/06/15 Pct Recovery = 58% Analysis Date = 10/06/15 Pct Recovery = 58% Analysis Date = 10/01/15 Pct Recovery = 58% Analysis Date = 10/01/15 Pct Recovery = 58% Analysis Date = 09/26/15 Pct Recovery = 58% Analysis Date = 09/26/15 Pct Recovery = 58% Analysis Date = 09/21/15 Pct Recovery = 58% Analysis Date = 09/21/15 Pct Recovery = 58% Analysis Date = 09/16/15 Pct Recovery = 58% Analysis Date = 09/16/15 Pct Recovery = 58% Analysis Date = 09/11/15 Pct Recovery = 58% Analysis Date = 09/11/15 Pct Recovery = 58% Analysis Date = 09/05/15 Pct Recovery = 58% Analysis Date = 09/05/15 Pct Recovery = 58% Analysis Date = 08/31/15 Pct Recovery = 58% Analysis Date = 08/31/15 Pct Recovery = 58% Analysis Date = 08/26/15 Pct Recovery = 59% Analysis Date = 08/26/15 Pct Recovery = 59% Analysis Date = 08/21/15 Pct Recovery = 58% Analysis Date = 08/21/15 Pct Recovery = 58% Analysis Date = 08/16/15 Pct Recovery = 58% Analysis Date = 08/16/15 Pct Recovery = 58% Analysis Date = 08/11/15 Pct Recovery = 58% Analysis Date = 08/11/15 Pct Recovery = 58% Analysis Date = 08/06/15 Pct Recovery = 58% Analysis Date = 08/06/15 Pct Recovery = 58% Analysis Date = 08/01/15 Pct Recovery = 58% Analysis Date = 08/01/15 Pct Recovery = 58% Analysis Date = 07/27/15 Pct Recovery = 58% Analysis Date = 07/27/15 Pct Recovery = 58% Analysis Date = 07/22/15 Pct Recovery = 58% Analysis Date = 07/22/15 Pct Recovery = 58% Analysis Date = 07/17/15 Pct Recovery = 58% Analysis Date = 07/17/15 Pct Recovery = 58% Analysis Date = 07/12/15 Pct Recovery = 58% Analysis Date = 07/12/15 Pct Recovery = 58% Analysis Date = 07/07/15 Pct Recovery = 58% Analysis Date = 07/07/15 Pct Recovery = 58% Analysis Date = 07/02/15 Pct Recovery = 58% Analysis Date = 07/02/15 Pct Recovery = 58% Analysis Date = 06/27/15 Pct Recovery = 58% Analysis Date = 06/27/15 Pct Recovery = 58% Analysis Date = 06/22/15 Pct Recovery = 58% Analysis Date = 06/22/15 Pct Recovery = 58% Analysis Date = 06/17/15 Pct Recovery = 58% Analysis Date = 06/17/15 Pct Recovery = 58% Analysis Date = 06/12/15 Pct Recovery = 58% Analysis Date = 06/12/15 Pct Recovery = 58% Analysis Date = 06/07/15 Pct Recovery = 58% Analysis Date = 06/07/15 Pct Recovery = 58% Analysis Date = 06/02/15 Pct Recovery = 58% Analysis Date = 06/02/15 Pct Recovery = 58% Analysis Date = 05/28/15 Pct Recovery = 58% Analysis Date = 05/28/15 Pct Recovery = 58% Analysis Date = 05/23/15 Pct Recovery = 58% Analysis Date = 05/23/15 Pct Recovery = 58% Analysis Date = 05/18/15 Pct Recovery = 58% Analysis Date = 05/18/15 Pct Recovery = 58% Analysis Date = 05/13/15 Pct Recovery = 58% Analysis Date = 05/13/15 Pct Recovery = 58% Analysis Date = 05/08/15 Pct Recovery = 58% Analysis Date = 05/08/15 Pct Recovery = 58% Analysis Date = 05/03/15 Pct Recovery = 58% Analysis Date = 05/03/15 Pct Recovery = 58% Analysis Date = 04/28/15 Pct Recovery = 58% Analysis Date = 04/28/15 Pct Recovery = 58% Analysis Date = 04/23/15 Pct Recovery = 58% Analysis Date = 04/23/15 Pct Recovery = 58% Analysis Date = 04/18/15 Pct Recovery = 58% Analysis Date = 04/18/15 Pct Recovery = 58% Analysis Date = 04/13/15 Pct Recovery = 58% Analysis Date = 04/13/15 Pct Recovery = 58% Analysis Date = 04/08/15 Pct Recovery = 58% Analysis Date = 04/08/15 Pct Recovery = 58% Analysis Date = 04/03/15 Pct Recovery = 58% Analysis Date = 04/03/15 Pct Recovery = 58% Analysis Date = 03/29/15 Pct Recovery = 58% Analysis Date = 03/29/15 Pct Recovery = 58% Analysis Date = 03/24/15 Pct Recovery = 58% Analysis Date = 03/24/15 Pct Recovery = 58% Analysis Date = 03/19/15 Pct Recovery = 57% Analysis Date = 03/19/15 Pct Recovery = 57% Analysis Date = 03/14/15 Pct Recovery = 57% Analysis Date = 03/14/15 Pct Recovery = 57% Analysis Date = 03/09/15 Pct Recovery = 57% Analysis Date = 03/09/15 Pct Recovery = 57% Analysis Date = 03/04/15 Pct Recovery = 57% Analysis Date = 03/04/15 Pct Recovery = 57% Analysis Date = 02/27/15 Pct Recovery = 57% Analysis Date = 02/27/15 Pct Recovery = 57% Analysis Date = 02/22/15 Pct Recovery = 57% Analysis Date = 02/22/15 Pct Recovery = 57% Analysis Date = 02/17/15 Pct Recovery = 57% Analysis Date = 02/17/15 Pct Recovery = 57% Analysis Date = 02/12/15 Pct Recovery = 57% Analysis Date = 02/12/15 Pct Recovery = 57% Analysis Date = 02/07/15 Pct Recovery = 57% Analysis Date = 02/07/15 Pct Recovery = 57% Analysis Date = 02/02/15 Pct Recovery = 57% Analysis Date = 02/02/15 Pct Recovery = 57% Analysis Date = 01/28/15 Pct Recovery = 57% Analysis Date = 01/28/15 Pct Recovery = 57% Analysis Date = 01/23/15 Pct Recovery = 57% Analysis Date = 01/23/15 Pct Recovery = 57% Analysis Date = 01/18/15 Pct Recovery = 57% Analysis Date = 01/18/15 Pct Recovery = 57% Analysis Date = 01/13/15 Pct Recovery = 57% Analysis Date = 01/13/15 Pct Recovery = 57% Analysis Date = 01/08/15 Pct Recovery = 57% Analysis Date = 01/08/15 Pct Recovery = 57% Analysis Date = 01/03/15 Pct Recovery = 57% Analysis Date = 01/03/15 Pct Recovery = 57% Analysis Date = 12/29/14 Pct Recovery = 57% Analysis Date = 12/29/14 Pct Recovery = 57% Analysis Date = 12/24/14 Pct Recovery = 57% Analysis Date = 12/24/14 Pct Recovery = 57% Analysis Date = 12/19/14 Pct Recovery = 57% Analysis Date = 12/19/14 Pct Recovery = 57% Analysis Date = 12/14/14 Pct Recovery = 57% Analysis Date = 12/14/14 Pct Recovery = 57% Analysis Date = 12/09/14 Pct Recovery = 57% Analysis Date = 12/09/14 Pct Recovery = 57% Analysis Date = 12/04/14 Pct Recovery = 58% Analysis Date = 12/04/14 Pct Recovery = 58% Analysis Date = 11/29/14 Pct Recovery = 58% Analysis Date = 11/29/14 Pct Recovery = 58% Analysis Date = 11/24/14 Pct Recovery = 58% Analysis Date = 11/24/14 Pct Recovery = 58% Analysis Date = 11/19/14 Pct Recovery = 58% Analysis Date = 11/19/14 Pct Recovery = 58% Analysis Date = 11/14/14 Pct Recovery = 58% Analysis Date = 11/14/14 Pct Recovery = 58% Analysis Date = 11/09/14 Pct Recovery = 58% Analysis Date = 11/09/14 Pct Recovery = 58% Analysis Date = 11/04/14 Pct Recovery = 58% Analysis Date = 11/04/14 Pct Recovery = 58% Analysis Date = 10/30/14 Pct Recovery = 58% Analysis Date = 10/30/14 Pct Recovery = 58% Analysis Date = 10/25/14 Pct Recovery = 58% Analysis Date = 10/25/14 Pct Recovery = 58% Analysis Date = 10/20/14 Pct Recovery = 58% Analysis Date = 10/20/14 Pct Recovery = 58% Analysis Date = 10/15/14 Pct Recovery = 58% Analysis Date = 10/15/14 Pct Recovery = 58% Analysis Date = 10/10/14 Pct Recovery = 58% Analysis Date = 10/10/14 Pct Recovery = 58% Analysis Date = 10/05/14 Pct Recovery = 58% Analysis Date = 10/05/14 Pct Recovery = 58% Analysis Date = 09/30/14 Pct Recovery = 58% Analysis Date = 09/30/14 Pct Recovery = 58% Analysis Date = 09/25/14 Pct Recovery = 58% Analysis Date = 09/25/14 Pct Recovery = 58% Analysis Date = 09/20/14 Pct Recovery = 58% Analysis Date = 09/20/14 Pct Recovery = 58% Analysis Date = 09/15/14 Pct Recovery = 58% Analysis Date = 09/15/14 Pct Recovery = 58% Analysis Date = 09/10/14 Pct Recovery = 58% Analysis Date = 09/10/14 Pct Recovery = 58% Analysis Date = 09/05/14 Pct Recovery = 58% Analysis Date = 09/05/14 Pct Recovery = 58% Analysis Date = 08/31/14 Pct Recovery = 58% Analysis Date = 08/31/14 Pct Recovery = 58% Analysis Date = 08/26/14 Pct Recovery = 58% Analysis Date = 08/26/14 Pct Recovery = 58% Analysis Date = 08/21/14 Pct Recovery = 58% Analysis Date = 08/21/14 Pct Recovery = 58% Analysis Date = 08/16/14 Pct Recovery = 58% Analysis Date = 08/16/14 Pct Recovery = 58% Analysis Date = 08/11/14 Pct Recovery = 58% Analysis Date = 08/11/14 Pct Recovery = 58% Analysis Date = 08/06/14 Pct Recovery = 58% Analysis Date = 08/06/14 Pct Recovery = 58% Analysis Date = 08/01/14 Pct Recovery = 58% Analysis Date = 08/01/14 Pct Recovery = 58% Analysis Date = 07/27/14 Pct Recovery = 58% Analysis Date = 07/27/14 Pct Recovery = 58% Analysis Date = 07/22/14 Pct Recovery = 58% Analysis Date = 07/22/14 Pct Recovery = 58% Analysis Date = 07/17/14 Pct Recovery = 58% Analysis Date = 07/17/14 Pct Recovery = 58% Analysis Date = 07/12/14 Pct Recovery = 58% Analysis Date = 07/12/14 Pct Recovery = 58% Analysis Date = 07/07/14 Pct Recovery = 58% Analysis Date = 07/07/14 Pct Recovery = 58% Analysis Date = 07/02/14 Pct Recovery = 58% Analysis Date = 07/02/14 Pct Recovery = 58% Analysis Date = 06/27/14 Pct Recovery = 58% Analysis Date = 06/27/14 Pct Recovery = 58% Analysis Date = 06/22/14 Pct Recovery = 58% Analysis Date = 06/22/14 Pct Recovery = 58% Analysis Date = 06/17/14 Pct Recovery = 58% Analysis Date = 06/17/14 Pct Recovery = 58% Analysis Date = 06/12/14 Pct Recovery = 58% Analysis Date = 06/12/14 Pct Recovery = 58% Analysis Date = 06/07/14 Pct Recovery = 58% Analysis Date = 06/07/14 Pct Recovery = 58% Analysis Date = 06/02/14 Pct Recovery = 58% Analysis Date = 06/02/14 Pct Recovery = 58% Analysis Date = 05/28/14 Pct Recovery = 58% Analysis Date = 05/28/14 Pct Recovery = 58% Analysis Date = 05/23/14 Pct Recovery = 58% Analysis Date = 05/23/14 Pct Recovery = 58% Analysis Date = 05/18/14 Pct Recovery = 58% Analysis Date = 05/18/14 Pct Recovery = 58% Analysis Date = 05/13/14 Pct Recovery = 58% Analysis Date = 05/13/14 Pct Recovery = 58% Analysis Date = 05/08/14 Pct Recovery = 58% Analysis Date = 05/08/14 Pct Recovery = 58% Analysis Date = 05/03/14 Pct Recovery = 58% Analysis Date = 05/03/14 Pct Recovery = 58% Analysis Date = 04/28/14 Pct Recovery = 58% Analysis Date = 04/28/14 Pct Recovery = 58% Analysis Date = 04/23/14 Pct Recovery = 58% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
FLUOXETINE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 75 60% 14% 57% 11%
Total 75 60% 14% 57% 11%

Sample Statistics
FLUOXETINE

Characteristic N % % Basis
Plotted 75 96% Spiked
Estimated Values 65 83% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 78 .  
False Negatives 3 4% 3 out of 78
Not Spiked 37 .  
False Positives 0 0% 0 out of 37

BQS OBSP Determination:
FLUTICASONE PROPIONATE
METHOD: 2440 , TESTIDCODE: 67529LCM56
Open Data Set

Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 71% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 95% Analysis Date = 11/05/15 SpikeMix = ERA 0406-15-08: 80 µl & Abs 052215: 80 µl Pct Recovery = 40% Analysis Date = 11/04/15 SpikeMix = Abs 052215: 80 µl & Abs 050115: 80 µl Pct Recovery = 70% Analysis Date = 01/17/16 SpikeMix = ERA 0406-15-09: 80 µl & ERA 0406-15-07A: 80 µl Pct Recovery = 54% Analysis Date = 11/24/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 76% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 51% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 58% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 80% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 80% Analysis Date = 04/29/15 SpikeMix = ERA 0319-14-05: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 83% Analysis Date = 03/11/15 SpikeMix = ERA 0318-14-02: 15 µl & Abs 041714: 15 µl Pct Recovery = 73% Analysis Date = 02/06/15 SpikeMix = Abs 041814: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 74% Analysis Date = 12/06/14 SpikeMix = ERA 0318-14-02: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 77% Analysis Date = 10/11/14 SpikeMix = ERA 0318-14-02: 60 µl & ERA 0319-14-04: 60 µl Pct Recovery = 69% Analysis Date = 08/21/14 SpikeMix = ERA 0318-14-02: 60 µl & Abs 041714: 60 µl Pct Recovery = 70% Analysis Date = 07/26/14 SpikeMix = ERA 0319-14-05: 60 µl & ERA 0318-14-02: 60 µl Pct Recovery = 86% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 53% Analysis Date = 12/07/14 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 82% Analysis Date = 10/25/14 SpikeMix = Abs 041614: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 68% Analysis Date = 06/22/14 SpikeMix = Abs 041814: 60 µl & Abs 041614: 60 µl Pct Recovery = 100% Analysis Date = 06/11/14 SpikeMix = Abs 041614: 60 µl & Abs 041714: 60 µl Pct Recovery = 75% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-08: 40 µl & Abs 052215: 40 µl Pct Recovery = 47% Analysis Date = 02/23/16 SpikeMix = Abs 052215: 40 µl & Abs 050115: 40 µl Pct Recovery = 97% Analysis Date = 09/10/15 SpikeMix = Abs 052215: 40 µl & ERA 0406-15-07A: 40 µl Pct Recovery = 116% Analysis Date = 07/31/15 SpikeMix = Abs 051315: 40 µl & Abs 052215: 40 µl Pct Recovery = 77% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-08: 40 µl & ERA 0406-15-09: 40 µl Pct Recovery = 89% Analysis Date = 07/31/15 SpikeMix = ERA 0406-15-09: 40 µl & Abs 050115: 40 µl Pct Recovery = 112% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 55% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 63% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 61% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 59% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 40% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 53% Analysis Date = 12/07/14 SpikeMix = ERA 0318-14-02: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 65% Analysis Date = 11/04/14 SpikeMix = Abs 041814: 8 µl & ERA 0318-14-02: 8 µl Pct Recovery = 36% Analysis Date = 04/30/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 17% Analysis Date = 02/10/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 68% Analysis Date = 10/24/14 SpikeMix = ERA 0319-14-05: 8 µl & Abs 041614: 8 µl Pct Recovery = 48% Analysis Date = 10/10/14 SpikeMix = Abs 041814: 30 µl & ERA 0318-14-02: 30 µl Pct Recovery = 66% Analysis Date = 08/30/14 SpikeMix = ERA 0318-14-02: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 65% Analysis Date = 09/12/14 SpikeMix = Abs 041614: 30 µl & ERA 0319-14-04: 30 µl Pct Recovery = 39% Analysis Date = 07/13/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 47% Analysis Date = 06/28/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 50% Analysis Date = 05/30/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 92% Analysis Date = 05/17/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 107% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 42% Analysis Date = 02/23/16 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 74% Analysis Date = 11/24/15 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 46% Analysis Date = 09/09/15 SpikeMix = ERA 0406-15-08: 20 µl & Abs 052215: 20 µl Pct Recovery = 102% Analysis Date = 07/09/15 SpikeMix = Abs 050115: 20 µl & Abs 052215: 20 µl Pct Recovery = 65% Analysis Date = 06/26/15 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 54% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 73% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 69% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-08: 20 µl & ERA 0406-15-09: 20 µl Pct Recovery = 19% Analysis Date = 11/24/15 SpikeMix = ERA 0406-15-09: 20 µl & Abs 050115: 20 µl Pct Recovery = 63% Analysis Date = 04/09/16 SpikeMix = Abs 051315: 10 µl & ERA 0406-15-09: 10 µl Pct Recovery = 133% Analysis Date = 01/18/17 Pct Recovery = 65% Analysis Date = 01/14/17 Pct Recovery = 65% Analysis Date = 01/14/17 Pct Recovery = 65% Analysis Date = 01/09/17 Pct Recovery = 65% Analysis Date = 01/09/17 Pct Recovery = 65% Analysis Date = 01/04/17 Pct Recovery = 65% Analysis Date = 01/04/17 Pct Recovery = 65% Analysis Date = 12/30/16 Pct Recovery = 65% Analysis Date = 12/30/16 Pct Recovery = 65% Analysis Date = 12/25/16 Pct Recovery = 65% Analysis Date = 12/25/16 Pct Recovery = 65% Analysis Date = 12/20/16 Pct Recovery = 65% Analysis Date = 12/20/16 Pct Recovery = 65% Analysis Date = 12/15/16 Pct Recovery = 65% Analysis Date = 12/15/16 Pct Recovery = 65% Analysis Date = 12/10/16 Pct Recovery = 65% Analysis Date = 12/10/16 Pct Recovery = 65% Analysis Date = 12/05/16 Pct Recovery = 65% Analysis Date = 12/05/16 Pct Recovery = 65% Analysis Date = 12/01/16 Pct Recovery = 65% Analysis Date = 12/01/16 Pct Recovery = 65% Analysis Date = 11/26/16 Pct Recovery = 65% Analysis Date = 11/26/16 Pct Recovery = 65% Analysis Date = 11/21/16 Pct Recovery = 65% Analysis Date = 11/21/16 Pct Recovery = 65% Analysis Date = 11/16/16 Pct Recovery = 65% Analysis Date = 11/16/16 Pct Recovery = 65% Analysis Date = 11/11/16 Pct Recovery = 65% Analysis Date = 11/11/16 Pct Recovery = 65% Analysis Date = 11/06/16 Pct Recovery = 65% Analysis Date = 11/06/16 Pct Recovery = 65% Analysis Date = 11/01/16 Pct Recovery = 65% Analysis Date = 11/01/16 Pct Recovery = 65% Analysis Date = 10/27/16 Pct Recovery = 66% Analysis Date = 10/27/16 Pct Recovery = 66% Analysis Date = 10/22/16 Pct Recovery = 66% Analysis Date = 10/22/16 Pct Recovery = 66% Analysis Date = 10/18/16 Pct Recovery = 66% Analysis Date = 10/18/16 Pct Recovery = 66% Analysis Date = 10/13/16 Pct Recovery = 66% Analysis Date = 10/13/16 Pct Recovery = 66% Analysis Date = 10/08/16 Pct Recovery = 66% Analysis Date = 10/08/16 Pct Recovery = 66% Analysis Date = 10/03/16 Pct Recovery = 66% Analysis Date = 10/03/16 Pct Recovery = 66% Analysis Date = 09/28/16 Pct Recovery = 66% Analysis Date = 09/28/16 Pct Recovery = 66% Analysis Date = 09/23/16 Pct Recovery = 66% Analysis Date = 09/23/16 Pct Recovery = 66% Analysis Date = 09/18/16 Pct Recovery = 66% Analysis Date = 09/18/16 Pct Recovery = 66% Analysis Date = 09/13/16 Pct Recovery = 66% Analysis Date = 09/13/16 Pct Recovery = 66% Analysis Date = 09/08/16 Pct Recovery = 66% Analysis Date = 09/08/16 Pct Recovery = 66% Analysis Date = 09/04/16 Pct Recovery = 66% Analysis Date = 09/04/16 Pct Recovery = 66% Analysis Date = 08/30/16 Pct Recovery = 66% Analysis Date = 08/30/16 Pct Recovery = 66% Analysis Date = 08/25/16 Pct Recovery = 66% Analysis Date = 08/25/16 Pct Recovery = 66% Analysis Date = 08/20/16 Pct Recovery = 66% Analysis Date = 08/20/16 Pct Recovery = 66% Analysis Date = 08/15/16 Pct Recovery = 66% Analysis Date = 08/15/16 Pct Recovery = 66% Analysis Date = 08/10/16 Pct Recovery = 66% Analysis Date = 08/10/16 Pct Recovery = 66% Analysis Date = 08/05/16 Pct Recovery = 66% Analysis Date = 08/05/16 Pct Recovery = 66% Analysis Date = 07/31/16 Pct Recovery = 66% Analysis Date = 07/31/16 Pct Recovery = 66% Analysis Date = 07/26/16 Pct Recovery = 66% Analysis Date = 07/26/16 Pct Recovery = 66% Analysis Date = 07/22/16 Pct Recovery = 66% Analysis Date = 07/22/16 Pct Recovery = 66% Analysis Date = 07/17/16 Pct Recovery = 66% Analysis Date = 07/17/16 Pct Recovery = 66% Analysis Date = 07/12/16 Pct Recovery = 66% Analysis Date = 07/12/16 Pct Recovery = 66% Analysis Date = 07/07/16 Pct Recovery = 66% Analysis Date = 07/07/16 Pct Recovery = 66% Analysis Date = 07/02/16 Pct Recovery = 66% Analysis Date = 07/02/16 Pct Recovery = 66% Analysis Date = 06/27/16 Pct Recovery = 66% Analysis Date = 06/27/16 Pct Recovery = 66% Analysis Date = 06/22/16 Pct Recovery = 66% Analysis Date = 06/22/16 Pct Recovery = 66% Analysis Date = 06/17/16 Pct Recovery = 66% Analysis Date = 06/17/16 Pct Recovery = 66% Analysis Date = 06/12/16 Pct Recovery = 66% Analysis Date = 06/12/16 Pct Recovery = 66% Analysis Date = 06/08/16 Pct Recovery = 66% Analysis Date = 06/08/16 Pct Recovery = 66% Analysis Date = 06/03/16 Pct Recovery = 66% Analysis Date = 06/03/16 Pct Recovery = 66% Analysis Date = 05/29/16 Pct Recovery = 66% Analysis Date = 05/29/16 Pct Recovery = 66% Analysis Date = 05/24/16 Pct Recovery = 66% Analysis Date = 05/24/16 Pct Recovery = 66% Analysis Date = 05/19/16 Pct Recovery = 66% Analysis Date = 05/19/16 Pct Recovery = 66% Analysis Date = 05/14/16 Pct Recovery = 66% Analysis Date = 05/14/16 Pct Recovery = 66% Analysis Date = 05/09/16 Pct Recovery = 66% Analysis Date = 05/09/16 Pct Recovery = 66% Analysis Date = 05/04/16 Pct Recovery = 66% Analysis Date = 05/04/16 Pct Recovery = 66% Analysis Date = 04/29/16 Pct Recovery = 66% Analysis Date = 04/29/16 Pct Recovery = 66% Analysis Date = 04/25/16 Pct Recovery = 66% Analysis Date = 04/25/16 Pct Recovery = 66% Analysis Date = 04/20/16 Pct Recovery = 66% Analysis Date = 04/20/16 Pct Recovery = 66% Analysis Date = 04/15/16 Pct Recovery = 66% Analysis Date = 04/15/16 Pct Recovery = 66% Analysis Date = 04/10/16 Pct Recovery = 66% Analysis Date = 04/10/16 Pct Recovery = 66% Analysis Date = 04/05/16 Pct Recovery = 67% Analysis Date = 04/05/16 Pct Recovery = 67% Analysis Date = 03/31/16 Pct Recovery = 67% Analysis Date = 03/31/16 Pct Recovery = 67% Analysis Date = 03/26/16 Pct Recovery = 67% Analysis Date = 03/26/16 Pct Recovery = 67% Analysis Date = 03/21/16 Pct Recovery = 67% Analysis Date = 03/21/16 Pct Recovery = 67% Analysis Date = 03/16/16 Pct Recovery = 67% Analysis Date = 03/16/16 Pct Recovery = 67% Analysis Date = 03/12/16 Pct Recovery = 68% Analysis Date = 03/12/16 Pct Recovery = 68% Analysis Date = 03/07/16 Pct Recovery = 68% Analysis Date = 03/07/16 Pct Recovery = 68% Analysis Date = 03/02/16 Pct Recovery = 68% Analysis Date = 03/02/16 Pct Recovery = 68% Analysis Date = 02/26/16 Pct Recovery = 68% Analysis Date = 02/26/16 Pct Recovery = 68% Analysis Date = 02/21/16 Pct Recovery = 68% Analysis Date = 02/21/16 Pct Recovery = 68% Analysis Date = 02/16/16 Pct Recovery = 69% Analysis Date = 02/16/16 Pct Recovery = 69% Analysis Date = 02/11/16 Pct Recovery = 69% Analysis Date = 02/11/16 Pct Recovery = 69% Analysis Date = 02/06/16 Pct Recovery = 69% Analysis Date = 02/06/16 Pct Recovery = 69% Analysis Date = 02/01/16 Pct Recovery = 69% Analysis Date = 02/01/16 Pct Recovery = 69% Analysis Date = 01/28/16 Pct Recovery = 69% Analysis Date = 01/28/16 Pct Recovery = 69% Analysis Date = 01/23/16 Pct Recovery = 69% Analysis Date = 01/23/16 Pct Recovery = 69% Analysis Date = 01/18/16 Pct Recovery = 70% Analysis Date = 01/18/16 Pct Recovery = 70% Analysis Date = 01/13/16 Pct Recovery = 70% Analysis Date = 01/13/16 Pct Recovery = 70% Analysis Date = 01/08/16 Pct Recovery = 70% Analysis Date = 01/08/16 Pct Recovery = 70% Analysis Date = 01/03/16 Pct Recovery = 70% Analysis Date = 01/03/16 Pct Recovery = 70% Analysis Date = 12/29/15 Pct Recovery = 70% Analysis Date = 12/29/15 Pct Recovery = 70% Analysis Date = 12/24/15 Pct Recovery = 70% Analysis Date = 12/24/15 Pct Recovery = 70% Analysis Date = 12/19/15 Pct Recovery = 71% Analysis Date = 12/19/15 Pct Recovery = 71% Analysis Date = 12/15/15 Pct Recovery = 71% Analysis Date = 12/15/15 Pct Recovery = 71% Analysis Date = 12/10/15 Pct Recovery = 71% Analysis Date = 12/10/15 Pct Recovery = 71% Analysis Date = 12/05/15 Pct Recovery = 71% Analysis Date = 12/05/15 Pct Recovery = 71% Analysis Date = 11/30/15 Pct Recovery = 71% Analysis Date = 11/30/15 Pct Recovery = 71% Analysis Date = 11/25/15 Pct Recovery = 71% Analysis Date = 11/25/15 Pct Recovery = 71% Analysis Date = 11/20/15 Pct Recovery = 71% Analysis Date = 11/20/15 Pct Recovery = 71% Analysis Date = 11/15/15 Pct Recovery = 71% Analysis Date = 11/15/15 Pct Recovery = 71% Analysis Date = 11/10/15 Pct Recovery = 71% Analysis Date = 11/10/15 Pct Recovery = 71% Analysis Date = 11/05/15 Pct Recovery = 71% Analysis Date = 11/05/15 Pct Recovery = 71% Analysis Date = 11/01/15 Pct Recovery = 71% Analysis Date = 11/01/15 Pct Recovery = 71% Analysis Date = 10/27/15 Pct Recovery = 71% Analysis Date = 10/27/15 Pct Recovery = 71% Analysis Date = 10/22/15 Pct Recovery = 71% Analysis Date = 10/22/15 Pct Recovery = 71% Analysis Date = 10/17/15 Pct Recovery = 71% Analysis Date = 10/17/15 Pct Recovery = 71% Analysis Date = 10/12/15 Pct Recovery = 71% Analysis Date = 10/12/15 Pct Recovery = 71% Analysis Date = 10/07/15 Pct Recovery = 70% Analysis Date = 10/07/15 Pct Recovery = 70% Analysis Date = 10/02/15 Pct Recovery = 70% Analysis Date = 10/02/15 Pct Recovery = 70% Analysis Date = 09/27/15 Pct Recovery = 70% Analysis Date = 09/27/15 Pct Recovery = 70% Analysis Date = 09/22/15 Pct Recovery = 70% Analysis Date = 09/22/15 Pct Recovery = 70% Analysis Date = 09/17/15 Pct Recovery = 70% Analysis Date = 09/17/15 Pct Recovery = 70% Analysis Date = 09/13/15 Pct Recovery = 70% Analysis Date = 09/13/15 Pct Recovery = 70% Analysis Date = 09/08/15 Pct Recovery = 70% Analysis Date = 09/08/15 Pct Recovery = 70% Analysis Date = 09/03/15 Pct Recovery = 70% Analysis Date = 09/03/15 Pct Recovery = 70% Analysis Date = 08/29/15 Pct Recovery = 70% Analysis Date = 08/29/15 Pct Recovery = 70% Analysis Date = 08/24/15 Pct Recovery = 70% Analysis Date = 08/24/15 Pct Recovery = 70% Analysis Date = 08/19/15 Pct Recovery = 70% Analysis Date = 08/19/15 Pct Recovery = 70% Analysis Date = 08/14/15 Pct Recovery = 70% Analysis Date = 08/14/15 Pct Recovery = 70% Analysis Date = 08/09/15 Pct Recovery = 70% Analysis Date = 08/09/15 Pct Recovery = 70% Analysis Date = 08/04/15 Pct Recovery = 70% Analysis Date = 08/04/15 Pct Recovery = 70% Analysis Date = 07/31/15 Pct Recovery = 70% Analysis Date = 07/31/15 Pct Recovery = 70% Analysis Date = 07/26/15 Pct Recovery = 70% Analysis Date = 07/26/15 Pct Recovery = 70% Analysis Date = 07/21/15 Pct Recovery = 70% Analysis Date = 07/21/15 Pct Recovery = 70% Analysis Date = 07/16/15 Pct Recovery = 70% Analysis Date = 07/16/15 Pct Recovery = 70% Analysis Date = 07/11/15 Pct Recovery = 70% Analysis Date = 07/11/15 Pct Recovery = 70% Analysis Date = 07/06/15 Pct Recovery = 70% Analysis Date = 07/06/15 Pct Recovery = 70% Analysis Date = 07/01/15 Pct Recovery = 70% Analysis Date = 07/01/15 Pct Recovery = 70% Analysis Date = 06/26/15 Pct Recovery = 70% Analysis Date = 06/26/15 Pct Recovery = 70% Analysis Date = 06/21/15 Pct Recovery = 70% Analysis Date = 06/21/15 Pct Recovery = 70% Analysis Date = 06/17/15 Pct Recovery = 70% Analysis Date = 06/17/15 Pct Recovery = 70% Analysis Date = 06/12/15 Pct Recovery = 70% Analysis Date = 06/12/15 Pct Recovery = 70% Analysis Date = 06/07/15 Pct Recovery = 70% Analysis Date = 06/07/15 Pct Recovery = 70% Analysis Date = 06/02/15 Pct Recovery = 69% Analysis Date = 06/02/15 Pct Recovery = 69% Analysis Date = 05/28/15 Pct Recovery = 69% Analysis Date = 05/28/15 Pct Recovery = 69% Analysis Date = 05/23/15 Pct Recovery = 69% Analysis Date = 05/23/15 Pct Recovery = 69% Analysis Date = 05/18/15 Pct Recovery = 69% Analysis Date = 05/18/15 Pct Recovery = 69% Analysis Date = 05/13/15 Pct Recovery = 69% Analysis Date = 05/13/15 Pct Recovery = 69% Analysis Date = 05/08/15 Pct Recovery = 69% Analysis Date = 05/08/15 Pct Recovery = 69% Analysis Date = 05/04/15 Pct Recovery = 69% Analysis Date = 05/04/15 Pct Recovery = 69% Analysis Date = 04/29/15 Pct Recovery = 69% Analysis Date = 04/29/15 Pct Recovery = 69% Analysis Date = 04/24/15 Pct Recovery = 69% Analysis Date = 04/24/15 Pct Recovery = 69% Analysis Date = 04/19/15 Pct Recovery = 69% Analysis Date = 04/19/15 Pct Recovery = 69% Analysis Date = 04/14/15 Pct Recovery = 69% Analysis Date = 04/14/15 Pct Recovery = 69% Analysis Date = 04/09/15 Pct Recovery = 69% Analysis Date = 04/09/15 Pct Recovery = 69% Analysis Date = 04/04/15 Pct Recovery = 68% Analysis Date = 04/04/15 Pct Recovery = 68% Analysis Date = 03/30/15 Pct Recovery = 68% Analysis Date = 03/30/15 Pct Recovery = 68% Analysis Date = 03/25/15 Pct Recovery = 68% Analysis Date = 03/25/15 Pct Recovery = 68% Analysis Date = 03/21/15 Pct Recovery = 68% Analysis Date = 03/21/15 Pct Recovery = 68% Analysis Date = 03/16/15 Pct Recovery = 68% Analysis Date = 03/16/15 Pct Recovery = 68% Analysis Date = 03/11/15 Pct Recovery = 68% Analysis Date = 03/11/15 Pct Recovery = 68% Analysis Date = 03/06/15 Pct Recovery = 68% Analysis Date = 03/06/15 Pct Recovery = 68% Analysis Date = 03/01/15 Pct Recovery = 67% Analysis Date = 03/01/15 Pct Recovery = 67% Analysis Date = 02/24/15 Pct Recovery = 67% Analysis Date = 02/24/15 Pct Recovery = 67% Analysis Date = 02/19/15 Pct Recovery = 67% Analysis Date = 02/19/15 Pct Recovery = 67% Analysis Date = 02/14/15 Pct Recovery = 67% Analysis Date = 02/14/15 Pct Recovery = 67% Analysis Date = 02/09/15 Pct Recovery = 66% Analysis Date = 02/09/15 Pct Recovery = 66% Analysis Date = 02/05/15 Pct Recovery = 66% Analysis Date = 02/05/15 Pct Recovery = 66% Analysis Date = 01/31/15 Pct Recovery = 66% Analysis Date = 01/31/15 Pct Recovery = 66% Analysis Date = 01/26/15 Pct Recovery = 66% Analysis Date = 01/26/15 Pct Recovery = 66% Analysis Date = 01/21/15 Pct Recovery = 66% Analysis Date = 01/21/15 Pct Recovery = 66% Analysis Date = 01/16/15 Pct Recovery = 67% Analysis Date = 01/16/15 Pct Recovery = 67% Analysis Date = 01/11/15 Pct Recovery = 67% Analysis Date = 01/11/15 Pct Recovery = 67% Analysis Date = 01/06/15 Pct Recovery = 67% Analysis Date = 01/06/15 Pct Recovery = 67% Analysis Date = 01/01/15 Pct Recovery = 67% Analysis Date = 01/01/15 Pct Recovery = 67% Analysis Date = 12/27/14 Pct Recovery = 67% Analysis Date = 12/27/14 Pct Recovery = 67% Analysis Date = 12/23/14 Pct Recovery = 67% Analysis Date = 12/23/14 Pct Recovery = 67% Analysis Date = 12/18/14 Pct Recovery = 67% Analysis Date = 12/18/14 Pct Recovery = 67% Analysis Date = 12/13/14 Pct Recovery = 67% Analysis Date = 12/13/14 Pct Recovery = 67% Analysis Date = 12/08/14 Pct Recovery = 67% Analysis Date = 12/08/14 Pct Recovery = 67% Analysis Date = 12/03/14 Pct Recovery = 67% Analysis Date = 12/03/14 Pct Recovery = 67% Analysis Date = 11/28/14 Pct Recovery = 67% Analysis Date = 11/28/14 Pct Recovery = 67% Analysis Date = 11/23/14 Pct Recovery = 67% Analysis Date = 11/23/14 Pct Recovery = 67% Analysis Date = 11/18/14 Pct Recovery = 67% Analysis Date = 11/18/14 Pct Recovery = 67% Analysis Date = 11/13/14 Pct Recovery = 68% Analysis Date = 11/13/14 Pct Recovery = 68% Analysis Date = 11/09/14 Pct Recovery = 68% Analysis Date = 11/09/14 Pct Recovery = 68% Analysis Date = 11/04/14 Pct Recovery = 68% Analysis Date = 11/04/14 Pct Recovery = 68% Analysis Date = 10/30/14 Pct Recovery = 68% Analysis Date = 10/30/14 Pct Recovery = 68% Analysis Date = 10/25/14 Pct Recovery = 68% Analysis Date = 10/25/14 Pct Recovery = 68% Analysis Date = 10/20/14 Pct Recovery = 68% Analysis Date = 10/20/14 Pct Recovery = 68% Analysis Date = 10/15/14 Pct Recovery = 68% Analysis Date = 10/15/14 Pct Recovery = 68% Analysis Date = 10/10/14 Pct Recovery = 69% Analysis Date = 10/10/14 Pct Recovery = 69% Analysis Date = 10/05/14 Pct Recovery = 69% Analysis Date = 10/05/14 Pct Recovery = 69% Analysis Date = 09/30/14 Pct Recovery = 69% Analysis Date = 09/30/14 Pct Recovery = 69% Analysis Date = 09/26/14 Pct Recovery = 69% Analysis Date = 09/26/14 Pct Recovery = 69% Analysis Date = 09/21/14 Pct Recovery = 69% Analysis Date = 09/21/14 Pct Recovery = 69% Analysis Date = 09/16/14 Pct Recovery = 70% Analysis Date = 09/16/14 Pct Recovery = 70% Analysis Date = 09/11/14 Pct Recovery = 70% Analysis Date = 09/11/14 Pct Recovery = 70% Analysis Date = 09/06/14 Pct Recovery = 70% Analysis Date = 09/06/14 Pct Recovery = 70% Analysis Date = 09/01/14 Pct Recovery = 70% Analysis Date = 09/01/14 Pct Recovery = 70% Analysis Date = 08/27/14 Pct Recovery = 70% Analysis Date = 08/27/14 Pct Recovery = 70% Analysis Date = 08/22/14 Pct Recovery = 70% Analysis Date = 08/22/14 Pct Recovery = 70% Analysis Date = 08/17/14 Pct Recovery = 71% Analysis Date = 08/17/14 Pct Recovery = 71% Analysis Date = 08/13/14 Pct Recovery = 71% Analysis Date = 08/13/14 Pct Recovery = 71% Analysis Date = 08/08/14 Pct Recovery = 71% Analysis Date = 08/08/14 Pct Recovery = 71% Analysis Date = 08/03/14 Pct Recovery = 71% Analysis Date = 08/03/14 Pct Recovery = 71% Analysis Date = 07/29/14 Pct Recovery = 72% Analysis Date = 07/29/14 Pct Recovery = 72% Analysis Date = 07/24/14 Pct Recovery = 72% Analysis Date = 07/24/14 Pct Recovery = 72% Analysis Date = 07/19/14 Pct Recovery = 72% Analysis Date = 07/19/14 Pct Recovery = 72% Analysis Date = 07/14/14 Pct Recovery = 72% Analysis Date = 07/14/14 Pct Recovery = 72% Analysis Date = 07/09/14 Pct Recovery = 72% Analysis Date = 07/09/14 Pct Recovery = 72% Analysis Date = 07/04/14 Pct Recovery = 73% Analysis Date = 07/04/14 Pct Recovery = 73% Analysis Date = 06/30/14 Pct Recovery = 73% Analysis Date = 06/30/14 Pct Recovery = 73% Analysis Date = 06/25/14 Pct Recovery = 73% Analysis Date = 06/25/14 Pct Recovery = 73% Analysis Date = 06/20/14 Pct Recovery = 73% Analysis Date = 06/20/14 Pct Recovery = 73% Analysis Date = 06/15/14 Pct Recovery = 74% Analysis Date = 06/15/14 Pct Recovery = 74% Analysis Date = 06/10/14 Pct Recovery = 74% Analysis Date = 06/10/14 Pct Recovery = 74% Analysis Date = 06/05/14 Pct Recovery = 74% Analysis Date = 06/05/14 Pct Recovery = 74% Analysis Date = 05/31/14 Pct Recovery = 74% Analysis Date = 05/31/14 Pct Recovery = 74% Analysis Date = 05/26/14 Pct Recovery = 75% Analysis Date = 05/26/14 Pct Recovery = 75% Analysis Date = 05/21/14 Pct Recovery = 75% Analysis Date = 05/21/14 Pct Recovery = 75% Analysis Date = 05/17/14 Pct Recovery = 75% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
FLUTICASONE PROPIONATE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 1 133% . 133% 0%
>= Reporting Level 56 67% 21% 68% 19%
Total 57 68% 23% 68% 20%

Sample Statistics
FLUTICASONE PROPIONATE

Characteristic N % % Basis
Plotted 57 88% Spiked
Estimated Values 14 22% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 4 6% Spiked
Spiked 65 .  
False Negatives 4 6% 4 out of 65
Not Spiked 50 .  
False Positives 0 0% 0 out of 50

BQS OBSP Determination:
FLUVOXAMINE
METHOD: 2440 , TESTIDCODE: 67521LCM56
Open Data Set

Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 43% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 39% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 80 µl & ERA 0406-15-08: 80 µl Pct Recovery = 52% Analysis Date = 11/04/15 SpikeMix = Abs 052215: 80 µl & Abs 050115: 80 µl Pct Recovery = 51% Analysis Date = 01/17/16 SpikeMix = ERA 0406-15-09: 80 µl & ERA 0406-15-07A: 80 µl Pct Recovery = 60% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 80 µl & Abs 051315: 80 µl Pct Recovery = 64% Analysis Date = 09/24/16 SpikeMix = Crescent EN160610015: 80 µl & Abs 061416: 80 µl Pct Recovery = 33% Analysis Date = 09/24/16 SpikeMix = Abs 061416: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 36% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 60% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 53% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 55% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 62% Analysis Date = 11/18/16 SpikeMix = ERA 04281604: 80 µl & ERA 04281603: 80 µl Pct Recovery = 35% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & ERA 04281604: 80 µl Pct Recovery = 31% Analysis Date = 04/29/15 SpikeMix = ERA 0319-14-05: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 63% Analysis Date = 03/11/15 SpikeMix = ERA 0318-14-02: 15 µl & Abs 041714: 15 µl Pct Recovery = 46% Analysis Date = 02/06/15 SpikeMix = Abs 041814: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 49% Analysis Date = 12/06/14 SpikeMix = ERA 0318-14-02: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 35% Analysis Date = 10/11/14 SpikeMix = ERA 0318-14-02: 60 µl & ERA 0319-14-04: 60 µl Pct Recovery = 50% Analysis Date = 08/21/14 SpikeMix = ERA 0318-14-02: 60 µl & Abs 041714: 60 µl Pct Recovery = 26% Analysis Date = 07/26/14 SpikeMix = ERA 0319-14-05: 60 µl & ERA 0318-14-02: 60 µl Pct Recovery = 47% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 37% Analysis Date = 12/07/14 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 41% Analysis Date = 10/25/14 SpikeMix = Abs 041614: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 26% Analysis Date = 06/22/14 SpikeMix = Abs 041814: 60 µl & Abs 041614: 60 µl Pct Recovery = 54% Analysis Date = 06/11/14 SpikeMix = Abs 041614: 60 µl & Abs 041714: 60 µl Pct Recovery = 28% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 54% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 51% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 48% Analysis Date = 02/23/16 SpikeMix = Abs 052215: 40 µl & Abs 050115: 40 µl Pct Recovery = 72% Analysis Date = 07/31/15 SpikeMix = ERA 0406-15-09: 40 µl & Abs 050115: 40 µl Pct Recovery = 62% Analysis Date = 07/30/15 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 58% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-07A: 40 µl & Abs 051315: 40 µl Pct Recovery = 46% Analysis Date = 11/04/15 SpikeMix = ERA 0406-15-07A: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 53% Analysis Date = 09/10/15 SpikeMix = Abs 052215: 40 µl & ERA 0406-15-07A: 40 µl Pct Recovery = 57% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 29% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 31% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 27% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 36% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 12% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 21% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 12% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 34% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 52% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 76% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 63% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 55% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 29% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 43% Analysis Date = 12/07/14 SpikeMix = ERA 0318-14-02: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 45% Analysis Date = 11/04/14 SpikeMix = Abs 041814: 8 µl & ERA 0318-14-02: 8 µl Pct Recovery = 11% Analysis Date = 04/30/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 37% Analysis Date = 02/10/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 24% Analysis Date = 10/24/14 SpikeMix = ERA 0319-14-05: 8 µl & Abs 041614: 8 µl Pct Recovery = 23% Analysis Date = 10/10/14 SpikeMix = Abs 041814: 30 µl & ERA 0318-14-02: 30 µl Pct Recovery = 45% Analysis Date = 08/30/14 SpikeMix = ERA 0318-14-02: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 43% Analysis Date = 07/20/14 SpikeMix = ERA 0318-14-02: 30 µl & Abs 041714: 30 µl Pct Recovery = 14% Analysis Date = 09/12/14 SpikeMix = Abs 041614: 30 µl & ERA 0319-14-04: 30 µl Pct Recovery = 35% Analysis Date = 07/13/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 25% Analysis Date = 06/28/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 32% Analysis Date = 05/30/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 34% Analysis Date = 05/17/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 40% Analysis Date = 04/23/14 SpikeMix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.2: 20 µl Pct Recovery = 44% Analysis Date = 11/25/15 SpikeMix = Abs 050115: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 36% Analysis Date = 11/24/15 SpikeMix = ERA 0406-15-09: 20 µl & Abs 050115: 20 µl Pct Recovery = 63% Analysis Date = 07/09/15 SpikeMix = Abs 050115: 20 µl & Abs 052215: 20 µl Pct Recovery = 56% Analysis Date = 06/09/15 SpikeMix = Abs 051315: 20 µl & Abs 050115: 20 µl Pct Recovery = 43% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 42% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 44% Analysis Date = 04/27/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 75% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 55% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 32% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 48% Analysis Date = 11/24/15 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 43% Analysis Date = 09/15/15 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 48% Analysis Date = 01/04/17 Pct Recovery = 38% Analysis Date = 12/31/16 Pct Recovery = 39% Analysis Date = 12/31/16 Pct Recovery = 39% Analysis Date = 12/26/16 Pct Recovery = 39% Analysis Date = 12/26/16 Pct Recovery = 39% Analysis Date = 12/21/16 Pct Recovery = 39% Analysis Date = 12/21/16 Pct Recovery = 39% Analysis Date = 12/16/16 Pct Recovery = 39% Analysis Date = 12/16/16 Pct Recovery = 39% Analysis Date = 12/11/16 Pct Recovery = 39% Analysis Date = 12/11/16 Pct Recovery = 39% Analysis Date = 12/06/16 Pct Recovery = 39% Analysis Date = 12/06/16 Pct Recovery = 39% Analysis Date = 12/01/16 Pct Recovery = 39% Analysis Date = 12/01/16 Pct Recovery = 39% Analysis Date = 11/26/16 Pct Recovery = 40% Analysis Date = 11/26/16 Pct Recovery = 40% Analysis Date = 11/21/16 Pct Recovery = 40% Analysis Date = 11/21/16 Pct Recovery = 40% Analysis Date = 11/16/16 Pct Recovery = 40% Analysis Date = 11/16/16 Pct Recovery = 40% Analysis Date = 11/11/16 Pct Recovery = 40% Analysis Date = 11/11/16 Pct Recovery = 40% Analysis Date = 11/06/16 Pct Recovery = 40% Analysis Date = 11/06/16 Pct Recovery = 40% Analysis Date = 11/01/16 Pct Recovery = 40% Analysis Date = 11/01/16 Pct Recovery = 40% Analysis Date = 10/27/16 Pct Recovery = 40% Analysis Date = 10/27/16 Pct Recovery = 40% Analysis Date = 10/22/16 Pct Recovery = 41% Analysis Date = 10/22/16 Pct Recovery = 41% Analysis Date = 10/17/16 Pct Recovery = 41% Analysis Date = 10/17/16 Pct Recovery = 41% Analysis Date = 10/13/16 Pct Recovery = 41% Analysis Date = 10/13/16 Pct Recovery = 41% Analysis Date = 10/08/16 Pct Recovery = 41% Analysis Date = 10/08/16 Pct Recovery = 41% Analysis Date = 10/03/16 Pct Recovery = 41% Analysis Date = 10/03/16 Pct Recovery = 41% Analysis Date = 09/28/16 Pct Recovery = 42% Analysis Date = 09/28/16 Pct Recovery = 42% Analysis Date = 09/23/16 Pct Recovery = 42% Analysis Date = 09/23/16 Pct Recovery = 42% Analysis Date = 09/18/16 Pct Recovery = 42% Analysis Date = 09/18/16 Pct Recovery = 42% Analysis Date = 09/13/16 Pct Recovery = 42% Analysis Date = 09/13/16 Pct Recovery = 42% Analysis Date = 09/08/16 Pct Recovery = 42% Analysis Date = 09/08/16 Pct Recovery = 42% Analysis Date = 09/03/16 Pct Recovery = 42% Analysis Date = 09/03/16 Pct Recovery = 42% Analysis Date = 08/29/16 Pct Recovery = 43% Analysis Date = 08/29/16 Pct Recovery = 43% Analysis Date = 08/24/16 Pct Recovery = 43% Analysis Date = 08/24/16 Pct Recovery = 43% Analysis Date = 08/19/16 Pct Recovery = 43% Analysis Date = 08/19/16 Pct Recovery = 43% Analysis Date = 08/14/16 Pct Recovery = 43% Analysis Date = 08/14/16 Pct Recovery = 43% Analysis Date = 08/09/16 Pct Recovery = 43% Analysis Date = 08/09/16 Pct Recovery = 43% Analysis Date = 08/04/16 Pct Recovery = 43% Analysis Date = 08/04/16 Pct Recovery = 43% Analysis Date = 07/30/16 Pct Recovery = 44% Analysis Date = 07/30/16 Pct Recovery = 44% Analysis Date = 07/25/16 Pct Recovery = 44% Analysis Date = 07/25/16 Pct Recovery = 44% Analysis Date = 07/21/16 Pct Recovery = 44% Analysis Date = 07/21/16 Pct Recovery = 44% Analysis Date = 07/16/16 Pct Recovery = 44% Analysis Date = 07/16/16 Pct Recovery = 44% Analysis Date = 07/11/16 Pct Recovery = 44% Analysis Date = 07/11/16 Pct Recovery = 44% Analysis Date = 07/06/16 Pct Recovery = 45% Analysis Date = 07/06/16 Pct Recovery = 45% Analysis Date = 07/01/16 Pct Recovery = 45% Analysis Date = 07/01/16 Pct Recovery = 45% Analysis Date = 06/26/16 Pct Recovery = 45% Analysis Date = 06/26/16 Pct Recovery = 45% Analysis Date = 06/21/16 Pct Recovery = 45% Analysis Date = 06/21/16 Pct Recovery = 45% Analysis Date = 06/16/16 Pct Recovery = 46% Analysis Date = 06/16/16 Pct Recovery = 46% Analysis Date = 06/11/16 Pct Recovery = 46% Analysis Date = 06/11/16 Pct Recovery = 46% Analysis Date = 06/06/16 Pct Recovery = 46% Analysis Date = 06/06/16 Pct Recovery = 46% Analysis Date = 06/01/16 Pct Recovery = 46% Analysis Date = 06/01/16 Pct Recovery = 46% Analysis Date = 05/27/16 Pct Recovery = 46% Analysis Date = 05/27/16 Pct Recovery = 46% Analysis Date = 05/22/16 Pct Recovery = 47% Analysis Date = 05/22/16 Pct Recovery = 47% Analysis Date = 05/17/16 Pct Recovery = 47% Analysis Date = 05/17/16 Pct Recovery = 47% Analysis Date = 05/12/16 Pct Recovery = 47% Analysis Date = 05/12/16 Pct Recovery = 47% Analysis Date = 05/07/16 Pct Recovery = 47% Analysis Date = 05/07/16 Pct Recovery = 47% Analysis Date = 05/02/16 Pct Recovery = 47% Analysis Date = 05/02/16 Pct Recovery = 47% Analysis Date = 04/28/16 Pct Recovery = 48% Analysis Date = 04/28/16 Pct Recovery = 48% Analysis Date = 04/23/16 Pct Recovery = 48% Analysis Date = 04/23/16 Pct Recovery = 48% Analysis Date = 04/18/16 Pct Recovery = 48% Analysis Date = 04/18/16 Pct Recovery = 48% Analysis Date = 04/13/16 Pct Recovery = 48% Analysis Date = 04/13/16 Pct Recovery = 48% Analysis Date = 04/08/16 Pct Recovery = 48% Analysis Date = 04/08/16 Pct Recovery = 48% Analysis Date = 04/03/16 Pct Recovery = 49% Analysis Date = 04/03/16 Pct Recovery = 49% Analysis Date = 03/29/16 Pct Recovery = 49% Analysis Date = 03/29/16 Pct Recovery = 49% Analysis Date = 03/24/16 Pct Recovery = 49% Analysis Date = 03/24/16 Pct Recovery = 49% Analysis Date = 03/19/16 Pct Recovery = 49% Analysis Date = 03/19/16 Pct Recovery = 49% Analysis Date = 03/14/16 Pct Recovery = 50% Analysis Date = 03/14/16 Pct Recovery = 50% Analysis Date = 03/09/16 Pct Recovery = 50% Analysis Date = 03/09/16 Pct Recovery = 50% Analysis Date = 03/04/16 Pct Recovery = 50% Analysis Date = 03/04/16 Pct Recovery = 50% Analysis Date = 02/28/16 Pct Recovery = 50% Analysis Date = 02/28/16 Pct Recovery = 50% Analysis Date = 02/23/16 Pct Recovery = 50% Analysis Date = 02/23/16 Pct Recovery = 50% Analysis Date = 02/18/16 Pct Recovery = 51% Analysis Date = 02/18/16 Pct Recovery = 51% Analysis Date = 02/13/16 Pct Recovery = 51% Analysis Date = 02/13/16 Pct Recovery = 51% Analysis Date = 02/09/16 Pct Recovery = 51% Analysis Date = 02/09/16 Pct Recovery = 51% Analysis Date = 02/04/16 Pct Recovery = 51% Analysis Date = 02/04/16 Pct Recovery = 51% Analysis Date = 01/30/16 Pct Recovery = 51% Analysis Date = 01/30/16 Pct Recovery = 51% Analysis Date = 01/25/16 Pct Recovery = 51% Analysis Date = 01/25/16 Pct Recovery = 51% Analysis Date = 01/20/16 Pct Recovery = 51% Analysis Date = 01/20/16 Pct Recovery = 51% Analysis Date = 01/15/16 Pct Recovery = 51% Analysis Date = 01/15/16 Pct Recovery = 51% Analysis Date = 01/10/16 Pct Recovery = 52% Analysis Date = 01/10/16 Pct Recovery = 52% Analysis Date = 01/05/16 Pct Recovery = 52% Analysis Date = 01/05/16 Pct Recovery = 52% Analysis Date = 12/31/15 Pct Recovery = 52% Analysis Date = 12/31/15 Pct Recovery = 52% Analysis Date = 12/26/15 Pct Recovery = 52% Analysis Date = 12/26/15 Pct Recovery = 52% Analysis Date = 12/21/15 Pct Recovery = 52% Analysis Date = 12/21/15 Pct Recovery = 52% Analysis Date = 12/16/15 Pct Recovery = 52% Analysis Date = 12/16/15 Pct Recovery = 52% Analysis Date = 12/11/15 Pct Recovery = 52% Analysis Date = 12/11/15 Pct Recovery = 52% Analysis Date = 12/06/15 Pct Recovery = 52% Analysis Date = 12/06/15 Pct Recovery = 52% Analysis Date = 12/01/15 Pct Recovery = 52% Analysis Date = 12/01/15 Pct Recovery = 52% Analysis Date = 11/26/15 Pct Recovery = 53% Analysis Date = 11/26/15 Pct Recovery = 53% Analysis Date = 11/21/15 Pct Recovery = 53% Analysis Date = 11/21/15 Pct Recovery = 53% Analysis Date = 11/17/15 Pct Recovery = 52% Analysis Date = 11/17/15 Pct Recovery = 52% Analysis Date = 11/12/15 Pct Recovery = 52% Analysis Date = 11/12/15 Pct Recovery = 52% Analysis Date = 11/07/15 Pct Recovery = 52% Analysis Date = 11/07/15 Pct Recovery = 52% Analysis Date = 11/02/15 Pct Recovery = 52% Analysis Date = 11/02/15 Pct Recovery = 52% Analysis Date = 10/28/15 Pct Recovery = 52% Analysis Date = 10/28/15 Pct Recovery = 52% Analysis Date = 10/23/15 Pct Recovery = 52% Analysis Date = 10/23/15 Pct Recovery = 52% Analysis Date = 10/18/15 Pct Recovery = 51% Analysis Date = 10/18/15 Pct Recovery = 51% Analysis Date = 10/13/15 Pct Recovery = 51% Analysis Date = 10/13/15 Pct Recovery = 51% Analysis Date = 10/08/15 Pct Recovery = 51% Analysis Date = 10/08/15 Pct Recovery = 51% Analysis Date = 10/03/15 Pct Recovery = 51% Analysis Date = 10/03/15 Pct Recovery = 51% Analysis Date = 09/28/15 Pct Recovery = 51% Analysis Date = 09/28/15 Pct Recovery = 51% Analysis Date = 09/23/15 Pct Recovery = 51% Analysis Date = 09/23/15 Pct Recovery = 51% Analysis Date = 09/18/15 Pct Recovery = 50% Analysis Date = 09/18/15 Pct Recovery = 50% Analysis Date = 09/13/15 Pct Recovery = 50% Analysis Date = 09/13/15 Pct Recovery = 50% Analysis Date = 09/08/15 Pct Recovery = 50% Analysis Date = 09/08/15 Pct Recovery = 50% Analysis Date = 09/03/15 Pct Recovery = 50% Analysis Date = 09/03/15 Pct Recovery = 50% Analysis Date = 08/29/15 Pct Recovery = 50% Analysis Date = 08/29/15 Pct Recovery = 50% Analysis Date = 08/25/15 Pct Recovery = 50% Analysis Date = 08/25/15 Pct Recovery = 50% Analysis Date = 08/20/15 Pct Recovery = 49% Analysis Date = 08/20/15 Pct Recovery = 49% Analysis Date = 08/15/15 Pct Recovery = 49% Analysis Date = 08/15/15 Pct Recovery = 49% Analysis Date = 08/10/15 Pct Recovery = 49% Analysis Date = 08/10/15 Pct Recovery = 49% Analysis Date = 08/05/15 Pct Recovery = 49% Analysis Date = 08/05/15 Pct Recovery = 49% Analysis Date = 07/31/15 Pct Recovery = 49% Analysis Date = 07/31/15 Pct Recovery = 49% Analysis Date = 07/26/15 Pct Recovery = 49% Analysis Date = 07/26/15 Pct Recovery = 49% Analysis Date = 07/21/15 Pct Recovery = 48% Analysis Date = 07/21/15 Pct Recovery = 48% Analysis Date = 07/16/15 Pct Recovery = 48% Analysis Date = 07/16/15 Pct Recovery = 48% Analysis Date = 07/11/15 Pct Recovery = 48% Analysis Date = 07/11/15 Pct Recovery = 48% Analysis Date = 07/06/15 Pct Recovery = 48% Analysis Date = 07/06/15 Pct Recovery = 48% Analysis Date = 07/01/15 Pct Recovery = 48% Analysis Date = 07/01/15 Pct Recovery = 48% Analysis Date = 06/26/15 Pct Recovery = 47% Analysis Date = 06/26/15 Pct Recovery = 47% Analysis Date = 06/21/15 Pct Recovery = 47% Analysis Date = 06/21/15 Pct Recovery = 47% Analysis Date = 06/16/15 Pct Recovery = 47% Analysis Date = 06/16/15 Pct Recovery = 47% Analysis Date = 06/11/15 Pct Recovery = 47% Analysis Date = 06/11/15 Pct Recovery = 47% Analysis Date = 06/07/15 Pct Recovery = 47% Analysis Date = 06/07/15 Pct Recovery = 47% Analysis Date = 06/02/15 Pct Recovery = 46% Analysis Date = 06/02/15 Pct Recovery = 46% Analysis Date = 05/28/15 Pct Recovery = 46% Analysis Date = 05/28/15 Pct Recovery = 46% Analysis Date = 05/23/15 Pct Recovery = 46% Analysis Date = 05/23/15 Pct Recovery = 46% Analysis Date = 05/18/15 Pct Recovery = 46% Analysis Date = 05/18/15 Pct Recovery = 46% Analysis Date = 05/13/15 Pct Recovery = 46% Analysis Date = 05/13/15 Pct Recovery = 46% Analysis Date = 05/08/15 Pct Recovery = 45% Analysis Date = 05/08/15 Pct Recovery = 45% Analysis Date = 05/03/15 Pct Recovery = 45% Analysis Date = 05/03/15 Pct Recovery = 45% Analysis Date = 04/28/15 Pct Recovery = 45% Analysis Date = 04/28/15 Pct Recovery = 45% Analysis Date = 04/23/15 Pct Recovery = 45% Analysis Date = 04/23/15 Pct Recovery = 45% Analysis Date = 04/18/15 Pct Recovery = 45% Analysis Date = 04/18/15 Pct Recovery = 45% Analysis Date = 04/13/15 Pct Recovery = 44% Analysis Date = 04/13/15 Pct Recovery = 44% Analysis Date = 04/08/15 Pct Recovery = 44% Analysis Date = 04/08/15 Pct Recovery = 44% Analysis Date = 04/03/15 Pct Recovery = 44% Analysis Date = 04/03/15 Pct Recovery = 44% Analysis Date = 03/29/15 Pct Recovery = 44% Analysis Date = 03/29/15 Pct Recovery = 44% Analysis Date = 03/24/15 Pct Recovery = 44% Analysis Date = 03/24/15 Pct Recovery = 44% Analysis Date = 03/19/15 Pct Recovery = 43% Analysis Date = 03/19/15 Pct Recovery = 43% Analysis Date = 03/15/15 Pct Recovery = 43% Analysis Date = 03/15/15 Pct Recovery = 43% Analysis Date = 03/10/15 Pct Recovery = 43% Analysis Date = 03/10/15 Pct Recovery = 43% Analysis Date = 03/05/15 Pct Recovery = 43% Analysis Date = 03/05/15 Pct Recovery = 43% Analysis Date = 02/28/15 Pct Recovery = 43% Analysis Date = 02/28/15 Pct Recovery = 43% Analysis Date = 02/23/15 Pct Recovery = 42% Analysis Date = 02/23/15 Pct Recovery = 42% Analysis Date = 02/18/15 Pct Recovery = 42% Analysis Date = 02/18/15 Pct Recovery = 42% Analysis Date = 02/13/15 Pct Recovery = 42% Analysis Date = 02/13/15 Pct Recovery = 42% Analysis Date = 02/08/15 Pct Recovery = 42% Analysis Date = 02/08/15 Pct Recovery = 42% Analysis Date = 02/03/15 Pct Recovery = 42% Analysis Date = 02/03/15 Pct Recovery = 42% Analysis Date = 01/29/15 Pct Recovery = 42% Analysis Date = 01/29/15 Pct Recovery = 42% Analysis Date = 01/24/15 Pct Recovery = 41% Analysis Date = 01/24/15 Pct Recovery = 41% Analysis Date = 01/19/15 Pct Recovery = 41% Analysis Date = 01/19/15 Pct Recovery = 41% Analysis Date = 01/14/15 Pct Recovery = 41% Analysis Date = 01/14/15 Pct Recovery = 41% Analysis Date = 01/09/15 Pct Recovery = 41% Analysis Date = 01/09/15 Pct Recovery = 41% Analysis Date = 01/04/15 Pct Recovery = 41% Analysis Date = 01/04/15 Pct Recovery = 41% Analysis Date = 12/30/14 Pct Recovery = 40% Analysis Date = 12/30/14 Pct Recovery = 40% Analysis Date = 12/25/14 Pct Recovery = 40% Analysis Date = 12/25/14 Pct Recovery = 40% Analysis Date = 12/21/14 Pct Recovery = 40% Analysis Date = 12/21/14 Pct Recovery = 40% Analysis Date = 12/16/14 Pct Recovery = 40% Analysis Date = 12/16/14 Pct Recovery = 40% Analysis Date = 12/11/14 Pct Recovery = 40% Analysis Date = 12/11/14 Pct Recovery = 40% Analysis Date = 12/06/14 Pct Recovery = 39% Analysis Date = 12/06/14 Pct Recovery = 39% Analysis Date = 12/01/14 Pct Recovery = 39% Analysis Date = 12/01/14 Pct Recovery = 39% Analysis Date = 11/26/14 Pct Recovery = 39% Analysis Date = 11/26/14 Pct Recovery = 39% Analysis Date = 11/21/14 Pct Recovery = 39% Analysis Date = 11/21/14 Pct Recovery = 39% Analysis Date = 11/16/14 Pct Recovery = 39% Analysis Date = 11/16/14 Pct Recovery = 39% Analysis Date = 11/11/14 Pct Recovery = 38% Analysis Date = 11/11/14 Pct Recovery = 38% Analysis Date = 11/06/14 Pct Recovery = 38% Analysis Date = 11/06/14 Pct Recovery = 38% Analysis Date = 11/01/14 Pct Recovery = 38% Analysis Date = 11/01/14 Pct Recovery = 38% Analysis Date = 10/27/14 Pct Recovery = 38% Analysis Date = 10/27/14 Pct Recovery = 38% Analysis Date = 10/22/14 Pct Recovery = 38% Analysis Date = 10/22/14 Pct Recovery = 38% Analysis Date = 10/17/14 Pct Recovery = 37% Analysis Date = 10/17/14 Pct Recovery = 37% Analysis Date = 10/12/14 Pct Recovery = 37% Analysis Date = 10/12/14 Pct Recovery = 37% Analysis Date = 10/07/14 Pct Recovery = 37% Analysis Date = 10/07/14 Pct Recovery = 37% Analysis Date = 10/03/14 Pct Recovery = 37% Analysis Date = 10/03/14 Pct Recovery = 37% Analysis Date = 09/28/14 Pct Recovery = 37% Analysis Date = 09/28/14 Pct Recovery = 37% Analysis Date = 09/23/14 Pct Recovery = 37% Analysis Date = 09/23/14 Pct Recovery = 37% Analysis Date = 09/18/14 Pct Recovery = 36% Analysis Date = 09/18/14 Pct Recovery = 36% Analysis Date = 09/13/14 Pct Recovery = 36% Analysis Date = 09/13/14 Pct Recovery = 36% Analysis Date = 09/08/14 Pct Recovery = 36% Analysis Date = 09/08/14 Pct Recovery = 36% Analysis Date = 09/03/14 Pct Recovery = 36% Analysis Date = 09/03/14 Pct Recovery = 36% Analysis Date = 08/29/14 Pct Recovery = 36% Analysis Date = 08/29/14 Pct Recovery = 36% Analysis Date = 08/24/14 Pct Recovery = 35% Analysis Date = 08/24/14 Pct Recovery = 35% Analysis Date = 08/19/14 Pct Recovery = 35% Analysis Date = 08/19/14 Pct Recovery = 35% Analysis Date = 08/14/14 Pct Recovery = 35% Analysis Date = 08/14/14 Pct Recovery = 35% Analysis Date = 08/09/14 Pct Recovery = 35% Analysis Date = 08/09/14 Pct Recovery = 35% Analysis Date = 08/04/14 Pct Recovery = 35% Analysis Date = 08/04/14 Pct Recovery = 35% Analysis Date = 07/30/14 Pct Recovery = 34% Analysis Date = 07/30/14 Pct Recovery = 34% Analysis Date = 07/25/14 Pct Recovery = 34% Analysis Date = 07/25/14 Pct Recovery = 34% Analysis Date = 07/20/14 Pct Recovery = 34% Analysis Date = 07/20/14 Pct Recovery = 34% Analysis Date = 07/15/14 Pct Recovery = 34% Analysis Date = 07/15/14 Pct Recovery = 34% Analysis Date = 07/11/14 Pct Recovery = 34% Analysis Date = 07/11/14 Pct Recovery = 34% Analysis Date = 07/06/14 Pct Recovery = 34% Analysis Date = 07/06/14 Pct Recovery = 34% Analysis Date = 07/01/14 Pct Recovery = 33% Analysis Date = 07/01/14 Pct Recovery = 33% Analysis Date = 06/26/14 Pct Recovery = 33% Analysis Date = 06/26/14 Pct Recovery = 33% Analysis Date = 06/21/14 Pct Recovery = 33% Analysis Date = 06/21/14 Pct Recovery = 33% Analysis Date = 06/16/14 Pct Recovery = 33% Analysis Date = 06/16/14 Pct Recovery = 33% Analysis Date = 06/11/14 Pct Recovery = 33% Analysis Date = 06/11/14 Pct Recovery = 33% Analysis Date = 06/06/14 Pct Recovery = 32% Analysis Date = 06/06/14 Pct Recovery = 32% Analysis Date = 06/01/14 Pct Recovery = 32% Analysis Date = 06/01/14 Pct Recovery = 32% Analysis Date = 05/27/14 Pct Recovery = 32% Analysis Date = 05/27/14 Pct Recovery = 32% Analysis Date = 05/22/14 Pct Recovery = 32% Analysis Date = 05/22/14 Pct Recovery = 32% Analysis Date = 05/17/14 Pct Recovery = 32% Analysis Date = 05/17/14 Pct Recovery = 32% Analysis Date = 05/12/14 Pct Recovery = 32% Analysis Date = 05/12/14 Pct Recovery = 32% Analysis Date = 05/07/14 Pct Recovery = 31% Analysis Date = 05/07/14 Pct Recovery = 31% Analysis Date = 05/02/14 Pct Recovery = 31% Analysis Date = 05/02/14 Pct Recovery = 31% Analysis Date = 04/27/14 Pct Recovery = 31% Analysis Date = 04/27/14 Pct Recovery = 31% Analysis Date = 04/23/14 Pct Recovery = 31% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
FLUVOXAMINE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 75 43% 15% 43% 15%
Total 75 43% 15% 43% 15%

Sample Statistics
FLUVOXAMINE

Characteristic N % % Basis
Plotted 75 96% Spiked
Estimated Values 75 96% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 78 .  
False Negatives 3 4% 3 out of 78
Not Spiked 37 .  
False Positives 0 0% 0 out of 37

BQS OBSP Determination:
GABAPENTIN
METHOD: 2440 , TESTIDCODE: 52817LCM56
Open Data Set

The SGPlot Procedure

Sample Statistics
GABAPENTIN

Characteristic N % % Basis
Plotted 0 . Spiked
Estimated Values 0 . Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 . Spiked
Spiked 0 .  
False Negatives 0 . 0 out of 0
Not Spiked 4 .  
False Positives 0 0% 0 out of 4

BQS OBSP Determination:
GLIPIZIDE
METHOD: 2440 , TESTIDCODE: 68001LCM56
Open Data Set

Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 75% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 71% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 80 µl & ERA 0406-15-08: 80 µl Pct Recovery = 99% Analysis Date = 11/04/15 SpikeMix = Abs 052215: 80 µl & Abs 050115: 80 µl Pct Recovery = 105% Analysis Date = 01/17/16 SpikeMix = ERA 0406-15-09: 80 µl & ERA 0406-15-07A: 80 µl Pct Recovery = 90% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 80 µl & Abs 051315: 80 µl Pct Recovery = 119% Analysis Date = 11/18/16 SpikeMix = ERA 04281604: 80 µl & ERA 04281603: 80 µl Pct Recovery = 79% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & ERA 04281604: 80 µl Pct Recovery = 78% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 71% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 72% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 81% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 82% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 99% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 98% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 121% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 103% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 94% Analysis Date = 02/23/16 SpikeMix = Abs 052215: 40 µl & Abs 050115: 40 µl Pct Recovery = 106% Analysis Date = 07/31/15 SpikeMix = ERA 0406-15-09: 40 µl & Abs 050115: 40 µl Pct Recovery = 113% Analysis Date = 07/30/15 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 97% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-07A: 40 µl & Abs 051315: 40 µl Pct Recovery = 85% Analysis Date = 11/04/15 SpikeMix = ERA 0406-15-07A: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 86% Analysis Date = 09/10/15 SpikeMix = Abs 052215: 40 µl & ERA 0406-15-07A: 40 µl Pct Recovery = 97% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 80% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 80% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 77% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 79% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 97% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 121% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 101% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 90% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 104% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 104% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 70% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 77% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 73% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 57% Analysis Date = 11/25/15 SpikeMix = Abs 050115: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 110% Analysis Date = 11/24/15 SpikeMix = ERA 0406-15-09: 20 µl & Abs 050115: 20 µl Pct Recovery = 106% Analysis Date = 08/27/15 SpikeMix = Abs 052215: 20 µl & Abs 050115: 20 µl Pct Recovery = 92% Analysis Date = 08/11/15 SpikeMix = Abs 050115: 20 µl & Abs 051315: 20 µl Pct Recovery = 74% Analysis Date = 07/09/15 SpikeMix = Abs 050115: 20 µl & Abs 052215: 20 µl Pct Recovery = 100% Analysis Date = 06/09/15 SpikeMix = Abs 051315: 20 µl & Abs 050115: 20 µl Pct Recovery = 87% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 73% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 75% Analysis Date = 04/27/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 132% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 94% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 112% Analysis Date = 11/24/15 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 95% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-09: 20 µl Pct Recovery = 27% Analysis Date = 09/15/15 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 92% Analysis Date = 06/23/14 SpikeMix = Abs 041814: 60 µl & Abs 041614: 60 µl Pct Recovery = 94% Analysis Date = 01/19/17 Pct Recovery = 87% Analysis Date = 01/14/17 Pct Recovery = 87% Analysis Date = 01/14/17 Pct Recovery = 87% Analysis Date = 01/09/17 Pct Recovery = 87% Analysis Date = 01/09/17 Pct Recovery = 87% Analysis Date = 01/04/17 Pct Recovery = 87% Analysis Date = 01/04/17 Pct Recovery = 87% Analysis Date = 12/31/16 Pct Recovery = 86% Analysis Date = 12/31/16 Pct Recovery = 86% Analysis Date = 12/26/16 Pct Recovery = 86% Analysis Date = 12/26/16 Pct Recovery = 86% Analysis Date = 12/21/16 Pct Recovery = 86% Analysis Date = 12/21/16 Pct Recovery = 86% Analysis Date = 12/17/16 Pct Recovery = 86% Analysis Date = 12/17/16 Pct Recovery = 86% Analysis Date = 12/12/16 Pct Recovery = 86% Analysis Date = 12/12/16 Pct Recovery = 86% Analysis Date = 12/07/16 Pct Recovery = 86% Analysis Date = 12/07/16 Pct Recovery = 86% Analysis Date = 12/02/16 Pct Recovery = 86% Analysis Date = 12/02/16 Pct Recovery = 86% Analysis Date = 11/28/16 Pct Recovery = 85% Analysis Date = 11/28/16 Pct Recovery = 85% Analysis Date = 11/23/16 Pct Recovery = 85% Analysis Date = 11/23/16 Pct Recovery = 85% Analysis Date = 11/18/16 Pct Recovery = 85% Analysis Date = 11/18/16 Pct Recovery = 85% Analysis Date = 11/14/16 Pct Recovery = 85% Analysis Date = 11/14/16 Pct Recovery = 85% Analysis Date = 11/09/16 Pct Recovery = 85% Analysis Date = 11/09/16 Pct Recovery = 85% Analysis Date = 11/04/16 Pct Recovery = 85% Analysis Date = 11/04/16 Pct Recovery = 85% Analysis Date = 10/31/16 Pct Recovery = 84% Analysis Date = 10/31/16 Pct Recovery = 84% Analysis Date = 10/26/16 Pct Recovery = 84% Analysis Date = 10/26/16 Pct Recovery = 84% Analysis Date = 10/21/16 Pct Recovery = 84% Analysis Date = 10/21/16 Pct Recovery = 84% Analysis Date = 10/16/16 Pct Recovery = 84% Analysis Date = 10/16/16 Pct Recovery = 84% Analysis Date = 10/12/16 Pct Recovery = 84% Analysis Date = 10/12/16 Pct Recovery = 84% Analysis Date = 10/07/16 Pct Recovery = 84% Analysis Date = 10/07/16 Pct Recovery = 84% Analysis Date = 10/02/16 Pct Recovery = 84% Analysis Date = 10/02/16 Pct Recovery = 84% Analysis Date = 09/28/16 Pct Recovery = 83% Analysis Date = 09/28/16 Pct Recovery = 83% Analysis Date = 09/23/16 Pct Recovery = 83% Analysis Date = 09/23/16 Pct Recovery = 83% Analysis Date = 09/18/16 Pct Recovery = 84% Analysis Date = 09/18/16 Pct Recovery = 84% Analysis Date = 09/13/16 Pct Recovery = 84% Analysis Date = 09/13/16 Pct Recovery = 84% Analysis Date = 09/09/16 Pct Recovery = 84% Analysis Date = 09/09/16 Pct Recovery = 84% Analysis Date = 09/04/16 Pct Recovery = 84% Analysis Date = 09/04/16 Pct Recovery = 84% Analysis Date = 08/30/16 Pct Recovery = 84% Analysis Date = 08/30/16 Pct Recovery = 84% Analysis Date = 08/26/16 Pct Recovery = 85% Analysis Date = 08/26/16 Pct Recovery = 85% Analysis Date = 08/21/16 Pct Recovery = 85% Analysis Date = 08/21/16 Pct Recovery = 85% Analysis Date = 08/16/16 Pct Recovery = 85% Analysis Date = 08/16/16 Pct Recovery = 85% Analysis Date = 08/12/16 Pct Recovery = 86% Analysis Date = 08/12/16 Pct Recovery = 86% Analysis Date = 08/07/16 Pct Recovery = 86% Analysis Date = 08/07/16 Pct Recovery = 86% Analysis Date = 08/02/16 Pct Recovery = 87% Analysis Date = 08/02/16 Pct Recovery = 87% Analysis Date = 07/28/16 Pct Recovery = 88% Analysis Date = 07/28/16 Pct Recovery = 88% Analysis Date = 07/24/16 Pct Recovery = 88% Analysis Date = 07/24/16 Pct Recovery = 88% Analysis Date = 07/19/16 Pct Recovery = 89% Analysis Date = 07/19/16 Pct Recovery = 89% Analysis Date = 07/14/16 Pct Recovery = 89% Analysis Date = 07/14/16 Pct Recovery = 89% Analysis Date = 07/10/16 Pct Recovery = 90% Analysis Date = 07/10/16 Pct Recovery = 90% Analysis Date = 07/05/16 Pct Recovery = 90% Analysis Date = 07/05/16 Pct Recovery = 90% Analysis Date = 06/30/16 Pct Recovery = 90% Analysis Date = 06/30/16 Pct Recovery = 90% Analysis Date = 06/25/16 Pct Recovery = 91% Analysis Date = 06/25/16 Pct Recovery = 91% Analysis Date = 06/21/16 Pct Recovery = 91% Analysis Date = 06/21/16 Pct Recovery = 91% Analysis Date = 06/16/16 Pct Recovery = 92% Analysis Date = 06/16/16 Pct Recovery = 92% Analysis Date = 06/11/16 Pct Recovery = 92% Analysis Date = 06/11/16 Pct Recovery = 92% Analysis Date = 06/07/16 Pct Recovery = 93% Analysis Date = 06/07/16 Pct Recovery = 93% Analysis Date = 06/02/16 Pct Recovery = 93% Analysis Date = 06/02/16 Pct Recovery = 93% Analysis Date = 05/28/16 Pct Recovery = 93% Analysis Date = 05/28/16 Pct Recovery = 93% Analysis Date = 05/24/16 Pct Recovery = 94% Analysis Date = 05/24/16 Pct Recovery = 94% Analysis Date = 05/19/16 Pct Recovery = 94% Analysis Date = 05/19/16 Pct Recovery = 94% Analysis Date = 05/14/16 Pct Recovery = 95% Analysis Date = 05/14/16 Pct Recovery = 95% Analysis Date = 05/09/16 Pct Recovery = 95% Analysis Date = 05/09/16 Pct Recovery = 95% Analysis Date = 05/05/16 Pct Recovery = 95% Analysis Date = 05/05/16 Pct Recovery = 95% Analysis Date = 04/30/16 Pct Recovery = 96% Analysis Date = 04/30/16 Pct Recovery = 96% Analysis Date = 04/25/16 Pct Recovery = 96% Analysis Date = 04/25/16 Pct Recovery = 96% Analysis Date = 04/21/16 Pct Recovery = 96% Analysis Date = 04/21/16 Pct Recovery = 96% Analysis Date = 04/16/16 Pct Recovery = 96% Analysis Date = 04/16/16 Pct Recovery = 96% Analysis Date = 04/11/16 Pct Recovery = 97% Analysis Date = 04/11/16 Pct Recovery = 97% Analysis Date = 04/06/16 Pct Recovery = 97% Analysis Date = 04/06/16 Pct Recovery = 97% Analysis Date = 04/02/16 Pct Recovery = 97% Analysis Date = 04/02/16 Pct Recovery = 97% Analysis Date = 03/28/16 Pct Recovery = 97% Analysis Date = 03/28/16 Pct Recovery = 97% Analysis Date = 03/23/16 Pct Recovery = 97% Analysis Date = 03/23/16 Pct Recovery = 97% Analysis Date = 03/19/16 Pct Recovery = 97% Analysis Date = 03/19/16 Pct Recovery = 97% Analysis Date = 03/14/16 Pct Recovery = 98% Analysis Date = 03/14/16 Pct Recovery = 98% Analysis Date = 03/09/16 Pct Recovery = 98% Analysis Date = 03/09/16 Pct Recovery = 98% Analysis Date = 03/05/16 Pct Recovery = 98% Analysis Date = 03/05/16 Pct Recovery = 98% Analysis Date = 02/29/16 Pct Recovery = 98% Analysis Date = 02/29/16 Pct Recovery = 98% Analysis Date = 02/24/16 Pct Recovery = 98% Analysis Date = 02/24/16 Pct Recovery = 98% Analysis Date = 02/19/16 Pct Recovery = 98% Analysis Date = 02/19/16 Pct Recovery = 98% Analysis Date = 02/15/16 Pct Recovery = 98% Analysis Date = 02/15/16 Pct Recovery = 98% Analysis Date = 02/10/16 Pct Recovery = 98% Analysis Date = 02/10/16 Pct Recovery = 98% Analysis Date = 02/05/16 Pct Recovery = 98% Analysis Date = 02/05/16 Pct Recovery = 98% Analysis Date = 02/01/16 Pct Recovery = 98% Analysis Date = 02/01/16 Pct Recovery = 98% Analysis Date = 01/27/16 Pct Recovery = 97% Analysis Date = 01/27/16 Pct Recovery = 97% Analysis Date = 01/22/16 Pct Recovery = 97% Analysis Date = 01/22/16 Pct Recovery = 97% Analysis Date = 01/18/16 Pct Recovery = 97% Analysis Date = 01/18/16 Pct Recovery = 97% Analysis Date = 01/13/16 Pct Recovery = 97% Analysis Date = 01/13/16 Pct Recovery = 97% Analysis Date = 01/08/16 Pct Recovery = 97% Analysis Date = 01/08/16 Pct Recovery = 97% Analysis Date = 01/03/16 Pct Recovery = 97% Analysis Date = 01/03/16 Pct Recovery = 97% Analysis Date = 12/30/15 Pct Recovery = 96% Analysis Date = 12/30/15 Pct Recovery = 96% Analysis Date = 12/25/15 Pct Recovery = 96% Analysis Date = 12/25/15 Pct Recovery = 96% Analysis Date = 12/20/15 Pct Recovery = 96% Analysis Date = 12/20/15 Pct Recovery = 96% Analysis Date = 12/16/15 Pct Recovery = 96% Analysis Date = 12/16/15 Pct Recovery = 96% Analysis Date = 12/11/15 Pct Recovery = 96% Analysis Date = 12/11/15 Pct Recovery = 96% Analysis Date = 12/06/15 Pct Recovery = 96% Analysis Date = 12/06/15 Pct Recovery = 96% Analysis Date = 12/01/15 Pct Recovery = 95% Analysis Date = 12/01/15 Pct Recovery = 95% Analysis Date = 11/27/15 Pct Recovery = 95% Analysis Date = 11/27/15 Pct Recovery = 95% Analysis Date = 11/22/15 Pct Recovery = 95% Analysis Date = 11/22/15 Pct Recovery = 95% Analysis Date = 11/17/15 Pct Recovery = 95% Analysis Date = 11/17/15 Pct Recovery = 95% Analysis Date = 11/13/15 Pct Recovery = 95% Analysis Date = 11/13/15 Pct Recovery = 95% Analysis Date = 11/08/15 Pct Recovery = 95% Analysis Date = 11/08/15 Pct Recovery = 95% Analysis Date = 11/03/15 Pct Recovery = 94% Analysis Date = 11/03/15 Pct Recovery = 94% Analysis Date = 10/30/15 Pct Recovery = 94% Analysis Date = 10/30/15 Pct Recovery = 94% Analysis Date = 10/25/15 Pct Recovery = 94% Analysis Date = 10/25/15 Pct Recovery = 94% Analysis Date = 10/20/15 Pct Recovery = 94% Analysis Date = 10/20/15 Pct Recovery = 94% Analysis Date = 10/15/15 Pct Recovery = 94% Analysis Date = 10/15/15 Pct Recovery = 94% Analysis Date = 10/11/15 Pct Recovery = 94% Analysis Date = 10/11/15 Pct Recovery = 94% Analysis Date = 10/06/15 Pct Recovery = 93% Analysis Date = 10/06/15 Pct Recovery = 93% Analysis Date = 10/01/15 Pct Recovery = 93% Analysis Date = 10/01/15 Pct Recovery = 93% Analysis Date = 09/27/15 Pct Recovery = 93% Analysis Date = 09/27/15 Pct Recovery = 93% Analysis Date = 09/22/15 Pct Recovery = 93% Analysis Date = 09/22/15 Pct Recovery = 93% Analysis Date = 09/17/15 Pct Recovery = 93% Analysis Date = 09/17/15 Pct Recovery = 93% Analysis Date = 09/12/15 Pct Recovery = 93% Analysis Date = 09/12/15 Pct Recovery = 93% Analysis Date = 09/08/15 Pct Recovery = 92% Analysis Date = 09/08/15 Pct Recovery = 92% Analysis Date = 09/03/15 Pct Recovery = 92% Analysis Date = 09/03/15 Pct Recovery = 92% Analysis Date = 08/29/15 Pct Recovery = 92% Analysis Date = 08/29/15 Pct Recovery = 92% Analysis Date = 08/25/15 Pct Recovery = 92% Analysis Date = 08/25/15 Pct Recovery = 92% Analysis Date = 08/20/15 Pct Recovery = 92% Analysis Date = 08/20/15 Pct Recovery = 92% Analysis Date = 08/15/15 Pct Recovery = 92% Analysis Date = 08/15/15 Pct Recovery = 92% Analysis Date = 08/11/15 Pct Recovery = 92% Analysis Date = 08/11/15 Pct Recovery = 92% Analysis Date = 08/06/15 Pct Recovery = 91% Analysis Date = 08/06/15 Pct Recovery = 91% Analysis Date = 08/01/15 Pct Recovery = 91% Analysis Date = 08/01/15 Pct Recovery = 91% Analysis Date = 07/27/15 Pct Recovery = 91% Analysis Date = 07/27/15 Pct Recovery = 91% Analysis Date = 07/23/15 Pct Recovery = 91% Analysis Date = 07/23/15 Pct Recovery = 91% Analysis Date = 07/18/15 Pct Recovery = 91% Analysis Date = 07/18/15 Pct Recovery = 91% Analysis Date = 07/13/15 Pct Recovery = 91% Analysis Date = 07/13/15 Pct Recovery = 91% Analysis Date = 07/09/15 Pct Recovery = 91% Analysis Date = 07/09/15 Pct Recovery = 91% Analysis Date = 07/04/15 Pct Recovery = 91% Analysis Date = 07/04/15 Pct Recovery = 91% Analysis Date = 06/29/15 Pct Recovery = 91% Analysis Date = 06/29/15 Pct Recovery = 91% Analysis Date = 06/24/15 Pct Recovery = 91% Analysis Date = 06/24/15 Pct Recovery = 91% Analysis Date = 06/20/15 Pct Recovery = 91% Analysis Date = 06/20/15 Pct Recovery = 91% Analysis Date = 06/15/15 Pct Recovery = 91% Analysis Date = 06/15/15 Pct Recovery = 91% Analysis Date = 06/10/15 Pct Recovery = 91% Analysis Date = 06/10/15 Pct Recovery = 91% Analysis Date = 06/06/15 Pct Recovery = 91% Analysis Date = 06/06/15 Pct Recovery = 91% Analysis Date = 06/01/15 Pct Recovery = 91% Analysis Date = 06/01/15 Pct Recovery = 91% Analysis Date = 05/27/15 Pct Recovery = 91% Analysis Date = 05/27/15 Pct Recovery = 91% Analysis Date = 05/23/15 Pct Recovery = 91% Analysis Date = 05/23/15 Pct Recovery = 91% Analysis Date = 05/18/15 Pct Recovery = 91% Analysis Date = 05/18/15 Pct Recovery = 91% Analysis Date = 05/13/15 Pct Recovery = 91% Analysis Date = 05/13/15 Pct Recovery = 91% Analysis Date = 05/08/15 Pct Recovery = 91% Analysis Date = 05/08/15 Pct Recovery = 91% Analysis Date = 05/04/15 Pct Recovery = 91% Analysis Date = 05/04/15 Pct Recovery = 91% Analysis Date = 04/29/15 Pct Recovery = 91% Analysis Date = 04/29/15 Pct Recovery = 91% Analysis Date = 04/24/15 Pct Recovery = 91% Analysis Date = 04/24/15 Pct Recovery = 91% Analysis Date = 04/20/15 Pct Recovery = 91% Analysis Date = 04/20/15 Pct Recovery = 91% Analysis Date = 04/15/15 Pct Recovery = 91% Analysis Date = 04/15/15 Pct Recovery = 91% Analysis Date = 04/10/15 Pct Recovery = 91% Analysis Date = 04/10/15 Pct Recovery = 91% Analysis Date = 04/06/15 Pct Recovery = 91% Analysis Date = 04/06/15 Pct Recovery = 91% Analysis Date = 04/01/15 Pct Recovery = 91% Analysis Date = 04/01/15 Pct Recovery = 91% Analysis Date = 03/27/15 Pct Recovery = 91% Analysis Date = 03/27/15 Pct Recovery = 91% Analysis Date = 03/22/15 Pct Recovery = 91% Analysis Date = 03/22/15 Pct Recovery = 91% Analysis Date = 03/18/15 Pct Recovery = 91% Analysis Date = 03/18/15 Pct Recovery = 91% Analysis Date = 03/13/15 Pct Recovery = 91% Analysis Date = 03/13/15 Pct Recovery = 91% Analysis Date = 03/08/15 Pct Recovery = 91% Analysis Date = 03/08/15 Pct Recovery = 91% Analysis Date = 03/04/15 Pct Recovery = 91% Analysis Date = 03/04/15 Pct Recovery = 91% Analysis Date = 02/27/15 Pct Recovery = 91% Analysis Date = 02/27/15 Pct Recovery = 91% Analysis Date = 02/22/15 Pct Recovery = 91% Analysis Date = 02/22/15 Pct Recovery = 91% Analysis Date = 02/17/15 Pct Recovery = 91% Analysis Date = 02/17/15 Pct Recovery = 91% Analysis Date = 02/13/15 Pct Recovery = 91% Analysis Date = 02/13/15 Pct Recovery = 91% Analysis Date = 02/08/15 Pct Recovery = 91% Analysis Date = 02/08/15 Pct Recovery = 91% Analysis Date = 02/03/15 Pct Recovery = 91% Analysis Date = 02/03/15 Pct Recovery = 91% Analysis Date = 01/30/15 Pct Recovery = 91% Analysis Date = 01/30/15 Pct Recovery = 91% Analysis Date = 01/25/15 Pct Recovery = 91% Analysis Date = 01/25/15 Pct Recovery = 91% Analysis Date = 01/20/15 Pct Recovery = 91% Analysis Date = 01/20/15 Pct Recovery = 91% Analysis Date = 01/16/15 Pct Recovery = 91% Analysis Date = 01/16/15 Pct Recovery = 91% Analysis Date = 01/11/15 Pct Recovery = 91% Analysis Date = 01/11/15 Pct Recovery = 91% Analysis Date = 01/06/15 Pct Recovery = 91% Analysis Date = 01/06/15 Pct Recovery = 91% Analysis Date = 01/01/15 Pct Recovery = 91% Analysis Date = 01/01/15 Pct Recovery = 91% Analysis Date = 12/28/14 Pct Recovery = 91% Analysis Date = 12/28/14 Pct Recovery = 91% Analysis Date = 12/23/14 Pct Recovery = 91% Analysis Date = 12/23/14 Pct Recovery = 91% Analysis Date = 12/18/14 Pct Recovery = 91% Analysis Date = 12/18/14 Pct Recovery = 91% Analysis Date = 12/14/14 Pct Recovery = 91% Analysis Date = 12/14/14 Pct Recovery = 91% Analysis Date = 12/09/14 Pct Recovery = 91% Analysis Date = 12/09/14 Pct Recovery = 91% Analysis Date = 12/04/14 Pct Recovery = 91% Analysis Date = 12/04/14 Pct Recovery = 91% Analysis Date = 11/29/14 Pct Recovery = 91% Analysis Date = 11/29/14 Pct Recovery = 91% Analysis Date = 11/25/14 Pct Recovery = 91% Analysis Date = 11/25/14 Pct Recovery = 91% Analysis Date = 11/20/14 Pct Recovery = 91% Analysis Date = 11/20/14 Pct Recovery = 91% Analysis Date = 11/15/14 Pct Recovery = 91% Analysis Date = 11/15/14 Pct Recovery = 91% Analysis Date = 11/11/14 Pct Recovery = 91% Analysis Date = 11/11/14 Pct Recovery = 91% Analysis Date = 11/06/14 Pct Recovery = 91% Analysis Date = 11/06/14 Pct Recovery = 91% Analysis Date = 11/01/14 Pct Recovery = 91% Analysis Date = 11/01/14 Pct Recovery = 91% Analysis Date = 10/28/14 Pct Recovery = 91% Analysis Date = 10/28/14 Pct Recovery = 91% Analysis Date = 10/23/14 Pct Recovery = 91% Analysis Date = 10/23/14 Pct Recovery = 91% Analysis Date = 10/18/14 Pct Recovery = 91% Analysis Date = 10/18/14 Pct Recovery = 91% Analysis Date = 10/13/14 Pct Recovery = 91% Analysis Date = 10/13/14 Pct Recovery = 91% Analysis Date = 10/09/14 Pct Recovery = 91% Analysis Date = 10/09/14 Pct Recovery = 91% Analysis Date = 10/04/14 Pct Recovery = 91% Analysis Date = 10/04/14 Pct Recovery = 91% Analysis Date = 09/29/14 Pct Recovery = 91% Analysis Date = 09/29/14 Pct Recovery = 91% Analysis Date = 09/25/14 Pct Recovery = 91% Analysis Date = 09/25/14 Pct Recovery = 91% Analysis Date = 09/20/14 Pct Recovery = 91% Analysis Date = 09/20/14 Pct Recovery = 91% Analysis Date = 09/15/14 Pct Recovery = 91% Analysis Date = 09/15/14 Pct Recovery = 91% Analysis Date = 09/10/14 Pct Recovery = 91% Analysis Date = 09/10/14 Pct Recovery = 91% Analysis Date = 09/06/14 Pct Recovery = 91% Analysis Date = 09/06/14 Pct Recovery = 91% Analysis Date = 09/01/14 Pct Recovery = 91% Analysis Date = 09/01/14 Pct Recovery = 91% Analysis Date = 08/27/14 Pct Recovery = 91% Analysis Date = 08/27/14 Pct Recovery = 91% Analysis Date = 08/23/14 Pct Recovery = 91% Analysis Date = 08/23/14 Pct Recovery = 91% Analysis Date = 08/18/14 Pct Recovery = 91% Analysis Date = 08/18/14 Pct Recovery = 91% Analysis Date = 08/13/14 Pct Recovery = 91% Analysis Date = 08/13/14 Pct Recovery = 91% Analysis Date = 08/09/14 Pct Recovery = 91% Analysis Date = 08/09/14 Pct Recovery = 91% Analysis Date = 08/04/14 Pct Recovery = 91% Analysis Date = 08/04/14 Pct Recovery = 91% Analysis Date = 07/30/14 Pct Recovery = 91% Analysis Date = 07/30/14 Pct Recovery = 91% Analysis Date = 07/25/14 Pct Recovery = 91% Analysis Date = 07/25/14 Pct Recovery = 91% Analysis Date = 07/21/14 Pct Recovery = 91% Analysis Date = 07/21/14 Pct Recovery = 91% Analysis Date = 07/16/14 Pct Recovery = 91% Analysis Date = 07/16/14 Pct Recovery = 91% Analysis Date = 07/11/14 Pct Recovery = 91% Analysis Date = 07/11/14 Pct Recovery = 91% Analysis Date = 07/07/14 Pct Recovery = 91% Analysis Date = 07/07/14 Pct Recovery = 91% Analysis Date = 07/02/14 Pct Recovery = 91% Analysis Date = 07/02/14 Pct Recovery = 91% Analysis Date = 06/27/14 Pct Recovery = 91% Analysis Date = 06/27/14 Pct Recovery = 91% Analysis Date = 06/23/14 Pct Recovery = 91% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
GLIPIZIDE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 1 94% . 94% 0%
>= Reporting Level 51 90% 18% 92% 19%
Total 52 90% 18% 92% 18%

Sample Statistics
GLIPIZIDE

Characteristic N % % Basis
Plotted 52 68% Spiked
Estimated Values 27 35% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 24 31% Spiked
Spiked 77 .  
False Negatives 1 1% 1 out of 77
Not Spiked 38 .  
False Positives 0 0% 0 out of 38

BQS OBSP Determination:
GLYBURIDE
METHOD: 2440 , TESTIDCODE: 68002LCM56
Open Data Set

Analysis Date = 01/17/16 SpikeMix = ERA 0406-15-09: 80 µl & ERA 0406-15-07A: 80 µl Pct Recovery = 69% Analysis Date = 11/24/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 81% Analysis Date = 10/01/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 21% Analysis Date = 11/05/15 SpikeMix = ERA 0406-15-08: 80 µl & Abs 052215: 80 µl Pct Recovery = 73% Analysis Date = 11/04/15 SpikeMix = Abs 052215: 80 µl & Abs 050115: 80 µl Pct Recovery = 71% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 67% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 64% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 85% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 84% Analysis Date = 09/24/16 SpikeMix = Crescent EN160610015: 80 µl & Abs 061416: 80 µl Pct Recovery = 83% Analysis Date = 09/24/16 SpikeMix = Abs 061416: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 79% Analysis Date = 05/07/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 83% Analysis Date = 04/29/15 SpikeMix = ERA 0319-14-05: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 81% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 77% Analysis Date = 01/16/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 84% Analysis Date = 12/07/14 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 72% Analysis Date = 12/06/14 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 74% Analysis Date = 08/28/14 SpikeMix = ERA 0319-14-04: 60 µl & ERA 0319-14-05: 60 µl Pct Recovery = 65% Analysis Date = 07/26/14 SpikeMix = ERA 0319-14-05: 60 µl & ERA 0318-14-02: 60 µl Pct Recovery = 67% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-04: 15 µl & Abs 041814: 15 µl Pct Recovery = 79% Analysis Date = 02/06/15 SpikeMix = Abs 041814: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 95% Analysis Date = 07/12/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 61% Analysis Date = 06/22/14 SpikeMix = Abs 041814: 60 µl & Abs 041614: 60 µl Pct Recovery = 99% Analysis Date = 05/21/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 65% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-08: 40 µl & ERA 0406-15-09: 40 µl Pct Recovery = 76% Analysis Date = 07/31/15 SpikeMix = ERA 0406-15-09: 40 µl & Abs 050115: 40 µl Pct Recovery = 81% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-08: 40 µl & Abs 052215: 40 µl Pct Recovery = 75% Analysis Date = 02/23/16 SpikeMix = Abs 052215: 40 µl & Abs 050115: 40 µl Pct Recovery = 90% Analysis Date = 09/10/15 SpikeMix = Abs 052215: 40 µl & ERA 0406-15-07A: 40 µl Pct Recovery = 90% Analysis Date = 07/31/15 SpikeMix = Abs 051315: 40 µl & Abs 052215: 40 µl Pct Recovery = 63% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 67% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 64% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 64% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 57% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 31% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 32% Analysis Date = 04/23/14 SpikeMix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.2: 20 µl Pct Recovery = 72% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 86% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 82% Analysis Date = 11/04/14 SpikeMix = Abs 041714: 8 µl & ERA 0319-14-05: 8 µl Pct Recovery = 65% Analysis Date = 10/24/14 SpikeMix = ERA 0319-14-05: 8 µl & Abs 041614: 8 µl Pct Recovery = 80% Analysis Date = 04/10/15 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 62% Analysis Date = 11/04/14 SpikeMix = Abs 041814: 8 µl & ERA 0318-14-02: 8 µl Pct Recovery = 78% Analysis Date = 10/11/14 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 31% Analysis Date = 08/30/14 SpikeMix = ERA 0318-14-02: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 75% Analysis Date = 07/13/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 47% Analysis Date = 10/10/14 SpikeMix = Abs 041714: 30 µl & Abs 041814: 30 µl Pct Recovery = 38% Analysis Date = 10/10/14 SpikeMix = Abs 041814: 30 µl & ERA 0318-14-02: 30 µl Pct Recovery = 32% Analysis Date = 07/13/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 54% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 8% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 70% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-08: 20 µl & ERA 0406-15-09: 20 µl Pct Recovery = 53% Analysis Date = 11/24/15 SpikeMix = ERA 0406-15-09: 20 µl & Abs 050115: 20 µl Pct Recovery = 62% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 50% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 54% Analysis Date = 02/23/16 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 62% Analysis Date = 11/24/15 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 88% Analysis Date = 09/09/15 SpikeMix = ERA 0406-15-08: 20 µl & Abs 052215: 20 µl Pct Recovery = 86% Analysis Date = 07/09/15 SpikeMix = Abs 050115: 20 µl & Abs 052215: 20 µl Pct Recovery = 63% Analysis Date = 06/26/15 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 60% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 66% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 88% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 74% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 73% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 68% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 69% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 64% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 70% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 68% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 61% Analysis Date = 01/18/17 Pct Recovery = 73% Analysis Date = 01/13/17 Pct Recovery = 73% Analysis Date = 01/13/17 Pct Recovery = 73% Analysis Date = 01/08/17 Pct Recovery = 73% Analysis Date = 01/08/17 Pct Recovery = 73% Analysis Date = 01/03/17 Pct Recovery = 72% Analysis Date = 01/03/17 Pct Recovery = 72% Analysis Date = 12/29/16 Pct Recovery = 72% Analysis Date = 12/29/16 Pct Recovery = 72% Analysis Date = 12/24/16 Pct Recovery = 72% Analysis Date = 12/24/16 Pct Recovery = 72% Analysis Date = 12/19/16 Pct Recovery = 72% Analysis Date = 12/19/16 Pct Recovery = 72% Analysis Date = 12/14/16 Pct Recovery = 71% Analysis Date = 12/14/16 Pct Recovery = 71% Analysis Date = 12/09/16 Pct Recovery = 71% Analysis Date = 12/09/16 Pct Recovery = 71% Analysis Date = 12/04/16 Pct Recovery = 71% Analysis Date = 12/04/16 Pct Recovery = 71% Analysis Date = 11/29/16 Pct Recovery = 71% Analysis Date = 11/29/16 Pct Recovery = 71% Analysis Date = 11/24/16 Pct Recovery = 70% Analysis Date = 11/24/16 Pct Recovery = 70% Analysis Date = 11/19/16 Pct Recovery = 70% Analysis Date = 11/19/16 Pct Recovery = 70% Analysis Date = 11/14/16 Pct Recovery = 70% Analysis Date = 11/14/16 Pct Recovery = 70% Analysis Date = 11/09/16 Pct Recovery = 70% Analysis Date = 11/09/16 Pct Recovery = 70% Analysis Date = 11/04/16 Pct Recovery = 69% Analysis Date = 11/04/16 Pct Recovery = 69% Analysis Date = 10/30/16 Pct Recovery = 69% Analysis Date = 10/30/16 Pct Recovery = 69% Analysis Date = 10/25/16 Pct Recovery = 69% Analysis Date = 10/25/16 Pct Recovery = 69% Analysis Date = 10/20/16 Pct Recovery = 69% Analysis Date = 10/20/16 Pct Recovery = 69% Analysis Date = 10/15/16 Pct Recovery = 68% Analysis Date = 10/15/16 Pct Recovery = 68% Analysis Date = 10/10/16 Pct Recovery = 68% Analysis Date = 10/10/16 Pct Recovery = 68% Analysis Date = 10/05/16 Pct Recovery = 68% Analysis Date = 10/05/16 Pct Recovery = 68% Analysis Date = 09/30/16 Pct Recovery = 68% Analysis Date = 09/30/16 Pct Recovery = 68% Analysis Date = 09/25/16 Pct Recovery = 68% Analysis Date = 09/25/16 Pct Recovery = 68% Analysis Date = 09/20/16 Pct Recovery = 67% Analysis Date = 09/20/16 Pct Recovery = 67% Analysis Date = 09/15/16 Pct Recovery = 67% Analysis Date = 09/15/16 Pct Recovery = 67% Analysis Date = 09/10/16 Pct Recovery = 67% Analysis Date = 09/10/16 Pct Recovery = 67% Analysis Date = 09/05/16 Pct Recovery = 67% Analysis Date = 09/05/16 Pct Recovery = 67% Analysis Date = 08/31/16 Pct Recovery = 67% Analysis Date = 08/31/16 Pct Recovery = 67% Analysis Date = 08/26/16 Pct Recovery = 67% Analysis Date = 08/26/16 Pct Recovery = 67% Analysis Date = 08/21/16 Pct Recovery = 66% Analysis Date = 08/21/16 Pct Recovery = 66% Analysis Date = 08/16/16 Pct Recovery = 66% Analysis Date = 08/16/16 Pct Recovery = 66% Analysis Date = 08/11/16 Pct Recovery = 66% Analysis Date = 08/11/16 Pct Recovery = 66% Analysis Date = 08/06/16 Pct Recovery = 66% Analysis Date = 08/06/16 Pct Recovery = 66% Analysis Date = 08/01/16 Pct Recovery = 66% Analysis Date = 08/01/16 Pct Recovery = 66% Analysis Date = 07/27/16 Pct Recovery = 66% Analysis Date = 07/27/16 Pct Recovery = 66% Analysis Date = 07/22/16 Pct Recovery = 66% Analysis Date = 07/22/16 Pct Recovery = 66% Analysis Date = 07/17/16 Pct Recovery = 66% Analysis Date = 07/17/16 Pct Recovery = 66% Analysis Date = 07/12/16 Pct Recovery = 66% Analysis Date = 07/12/16 Pct Recovery = 66% Analysis Date = 07/07/16 Pct Recovery = 66% Analysis Date = 07/07/16 Pct Recovery = 66% Analysis Date = 07/02/16 Pct Recovery = 65% Analysis Date = 07/02/16 Pct Recovery = 65% Analysis Date = 06/27/16 Pct Recovery = 65% Analysis Date = 06/27/16 Pct Recovery = 65% Analysis Date = 06/22/16 Pct Recovery = 65% Analysis Date = 06/22/16 Pct Recovery = 65% Analysis Date = 06/17/16 Pct Recovery = 65% Analysis Date = 06/17/16 Pct Recovery = 65% Analysis Date = 06/12/16 Pct Recovery = 65% Analysis Date = 06/12/16 Pct Recovery = 65% Analysis Date = 06/07/16 Pct Recovery = 65% Analysis Date = 06/07/16 Pct Recovery = 65% Analysis Date = 06/02/16 Pct Recovery = 65% Analysis Date = 06/02/16 Pct Recovery = 65% Analysis Date = 05/28/16 Pct Recovery = 65% Analysis Date = 05/28/16 Pct Recovery = 65% Analysis Date = 05/23/16 Pct Recovery = 65% Analysis Date = 05/23/16 Pct Recovery = 65% Analysis Date = 05/18/16 Pct Recovery = 65% Analysis Date = 05/18/16 Pct Recovery = 65% Analysis Date = 05/13/16 Pct Recovery = 65% Analysis Date = 05/13/16 Pct Recovery = 65% Analysis Date = 05/08/16 Pct Recovery = 65% Analysis Date = 05/08/16 Pct Recovery = 65% Analysis Date = 05/03/16 Pct Recovery = 65% Analysis Date = 05/03/16 Pct Recovery = 65% Analysis Date = 04/28/16 Pct Recovery = 65% Analysis Date = 04/28/16 Pct Recovery = 65% Analysis Date = 04/23/16 Pct Recovery = 64% Analysis Date = 04/23/16 Pct Recovery = 64% Analysis Date = 04/18/16 Pct Recovery = 64% Analysis Date = 04/18/16 Pct Recovery = 64% Analysis Date = 04/13/16 Pct Recovery = 64% Analysis Date = 04/13/16 Pct Recovery = 64% Analysis Date = 04/08/16 Pct Recovery = 64% Analysis Date = 04/08/16 Pct Recovery = 64% Analysis Date = 04/03/16 Pct Recovery = 64% Analysis Date = 04/03/16 Pct Recovery = 64% Analysis Date = 03/29/16 Pct Recovery = 64% Analysis Date = 03/29/16 Pct Recovery = 64% Analysis Date = 03/24/16 Pct Recovery = 64% Analysis Date = 03/24/16 Pct Recovery = 64% Analysis Date = 03/19/16 Pct Recovery = 64% Analysis Date = 03/19/16 Pct Recovery = 64% Analysis Date = 03/14/16 Pct Recovery = 65% Analysis Date = 03/14/16 Pct Recovery = 65% Analysis Date = 03/09/16 Pct Recovery = 65% Analysis Date = 03/09/16 Pct Recovery = 65% Analysis Date = 03/04/16 Pct Recovery = 65% Analysis Date = 03/04/16 Pct Recovery = 65% Analysis Date = 02/28/16 Pct Recovery = 65% Analysis Date = 02/28/16 Pct Recovery = 65% Analysis Date = 02/23/16 Pct Recovery = 65% Analysis Date = 02/23/16 Pct Recovery = 65% Analysis Date = 02/18/16 Pct Recovery = 65% Analysis Date = 02/18/16 Pct Recovery = 65% Analysis Date = 02/13/16 Pct Recovery = 65% Analysis Date = 02/13/16 Pct Recovery = 65% Analysis Date = 02/08/16 Pct Recovery = 65% Analysis Date = 02/08/16 Pct Recovery = 65% Analysis Date = 02/03/16 Pct Recovery = 65% Analysis Date = 02/03/16 Pct Recovery = 65% Analysis Date = 01/29/16 Pct Recovery = 65% Analysis Date = 01/29/16 Pct Recovery = 65% Analysis Date = 01/24/16 Pct Recovery = 66% Analysis Date = 01/24/16 Pct Recovery = 66% Analysis Date = 01/19/16 Pct Recovery = 66% Analysis Date = 01/19/16 Pct Recovery = 66% Analysis Date = 01/14/16 Pct Recovery = 66% Analysis Date = 01/14/16 Pct Recovery = 66% Analysis Date = 01/09/16 Pct Recovery = 66% Analysis Date = 01/09/16 Pct Recovery = 66% Analysis Date = 01/04/16 Pct Recovery = 66% Analysis Date = 01/04/16 Pct Recovery = 66% Analysis Date = 12/30/15 Pct Recovery = 66% Analysis Date = 12/30/15 Pct Recovery = 66% Analysis Date = 12/25/15 Pct Recovery = 66% Analysis Date = 12/25/15 Pct Recovery = 66% Analysis Date = 12/20/15 Pct Recovery = 67% Analysis Date = 12/20/15 Pct Recovery = 67% Analysis Date = 12/15/15 Pct Recovery = 67% Analysis Date = 12/15/15 Pct Recovery = 67% Analysis Date = 12/10/15 Pct Recovery = 67% Analysis Date = 12/10/15 Pct Recovery = 67% Analysis Date = 12/05/15 Pct Recovery = 67% Analysis Date = 12/05/15 Pct Recovery = 67% Analysis Date = 11/30/15 Pct Recovery = 67% Analysis Date = 11/30/15 Pct Recovery = 67% Analysis Date = 11/25/15 Pct Recovery = 67% Analysis Date = 11/25/15 Pct Recovery = 67% Analysis Date = 11/20/15 Pct Recovery = 67% Analysis Date = 11/20/15 Pct Recovery = 67% Analysis Date = 11/15/15 Pct Recovery = 68% Analysis Date = 11/15/15 Pct Recovery = 68% Analysis Date = 11/10/15 Pct Recovery = 68% Analysis Date = 11/10/15 Pct Recovery = 68% Analysis Date = 11/05/15 Pct Recovery = 68% Analysis Date = 11/05/15 Pct Recovery = 68% Analysis Date = 10/31/15 Pct Recovery = 68% Analysis Date = 10/31/15 Pct Recovery = 68% Analysis Date = 10/26/15 Pct Recovery = 68% Analysis Date = 10/26/15 Pct Recovery = 68% Analysis Date = 10/21/15 Pct Recovery = 68% Analysis Date = 10/21/15 Pct Recovery = 68% Analysis Date = 10/16/15 Pct Recovery = 69% Analysis Date = 10/16/15 Pct Recovery = 69% Analysis Date = 10/11/15 Pct Recovery = 69% Analysis Date = 10/11/15 Pct Recovery = 69% Analysis Date = 10/06/15 Pct Recovery = 69% Analysis Date = 10/06/15 Pct Recovery = 69% Analysis Date = 10/01/15 Pct Recovery = 69% Analysis Date = 10/01/15 Pct Recovery = 69% Analysis Date = 09/26/15 Pct Recovery = 69% Analysis Date = 09/26/15 Pct Recovery = 69% Analysis Date = 09/21/15 Pct Recovery = 69% Analysis Date = 09/21/15 Pct Recovery = 69% Analysis Date = 09/16/15 Pct Recovery = 69% Analysis Date = 09/16/15 Pct Recovery = 69% Analysis Date = 09/11/15 Pct Recovery = 70% Analysis Date = 09/11/15 Pct Recovery = 70% Analysis Date = 09/05/15 Pct Recovery = 70% Analysis Date = 09/05/15 Pct Recovery = 70% Analysis Date = 08/31/15 Pct Recovery = 70% Analysis Date = 08/31/15 Pct Recovery = 70% Analysis Date = 08/26/15 Pct Recovery = 70% Analysis Date = 08/26/15 Pct Recovery = 70% Analysis Date = 08/21/15 Pct Recovery = 70% Analysis Date = 08/21/15 Pct Recovery = 70% Analysis Date = 08/16/15 Pct Recovery = 70% Analysis Date = 08/16/15 Pct Recovery = 70% Analysis Date = 08/11/15 Pct Recovery = 71% Analysis Date = 08/11/15 Pct Recovery = 71% Analysis Date = 08/06/15 Pct Recovery = 71% Analysis Date = 08/06/15 Pct Recovery = 71% Analysis Date = 08/01/15 Pct Recovery = 71% Analysis Date = 08/01/15 Pct Recovery = 71% Analysis Date = 07/27/15 Pct Recovery = 71% Analysis Date = 07/27/15 Pct Recovery = 71% Analysis Date = 07/22/15 Pct Recovery = 71% Analysis Date = 07/22/15 Pct Recovery = 71% Analysis Date = 07/17/15 Pct Recovery = 71% Analysis Date = 07/17/15 Pct Recovery = 71% Analysis Date = 07/12/15 Pct Recovery = 71% Analysis Date = 07/12/15 Pct Recovery = 71% Analysis Date = 07/07/15 Pct Recovery = 71% Analysis Date = 07/07/15 Pct Recovery = 71% Analysis Date = 07/02/15 Pct Recovery = 71% Analysis Date = 07/02/15 Pct Recovery = 71% Analysis Date = 06/27/15 Pct Recovery = 71% Analysis Date = 06/27/15 Pct Recovery = 71% Analysis Date = 06/22/15 Pct Recovery = 71% Analysis Date = 06/22/15 Pct Recovery = 71% Analysis Date = 06/17/15 Pct Recovery = 71% Analysis Date = 06/17/15 Pct Recovery = 71% Analysis Date = 06/12/15 Pct Recovery = 71% Analysis Date = 06/12/15 Pct Recovery = 71% Analysis Date = 06/07/15 Pct Recovery = 71% Analysis Date = 06/07/15 Pct Recovery = 71% Analysis Date = 06/02/15 Pct Recovery = 71% Analysis Date = 06/02/15 Pct Recovery = 71% Analysis Date = 05/28/15 Pct Recovery = 71% Analysis Date = 05/28/15 Pct Recovery = 71% Analysis Date = 05/23/15 Pct Recovery = 71% Analysis Date = 05/23/15 Pct Recovery = 71% Analysis Date = 05/18/15 Pct Recovery = 71% Analysis Date = 05/18/15 Pct Recovery = 71% Analysis Date = 05/13/15 Pct Recovery = 71% Analysis Date = 05/13/15 Pct Recovery = 71% Analysis Date = 05/08/15 Pct Recovery = 71% Analysis Date = 05/08/15 Pct Recovery = 71% Analysis Date = 05/03/15 Pct Recovery = 71% Analysis Date = 05/03/15 Pct Recovery = 71% Analysis Date = 04/28/15 Pct Recovery = 71% Analysis Date = 04/28/15 Pct Recovery = 71% Analysis Date = 04/23/15 Pct Recovery = 70% Analysis Date = 04/23/15 Pct Recovery = 70% Analysis Date = 04/18/15 Pct Recovery = 70% Analysis Date = 04/18/15 Pct Recovery = 70% Analysis Date = 04/13/15 Pct Recovery = 70% Analysis Date = 04/13/15 Pct Recovery = 70% Analysis Date = 04/08/15 Pct Recovery = 70% Analysis Date = 04/08/15 Pct Recovery = 70% Analysis Date = 04/03/15 Pct Recovery = 70% Analysis Date = 04/03/15 Pct Recovery = 70% Analysis Date = 03/29/15 Pct Recovery = 70% Analysis Date = 03/29/15 Pct Recovery = 70% Analysis Date = 03/24/15 Pct Recovery = 70% Analysis Date = 03/24/15 Pct Recovery = 70% Analysis Date = 03/19/15 Pct Recovery = 70% Analysis Date = 03/19/15 Pct Recovery = 70% Analysis Date = 03/14/15 Pct Recovery = 70% Analysis Date = 03/14/15 Pct Recovery = 70% Analysis Date = 03/09/15 Pct Recovery = 69% Analysis Date = 03/09/15 Pct Recovery = 69% Analysis Date = 03/04/15 Pct Recovery = 69% Analysis Date = 03/04/15 Pct Recovery = 69% Analysis Date = 02/27/15 Pct Recovery = 69% Analysis Date = 02/27/15 Pct Recovery = 69% Analysis Date = 02/22/15 Pct Recovery = 69% Analysis Date = 02/22/15 Pct Recovery = 69% Analysis Date = 02/17/15 Pct Recovery = 69% Analysis Date = 02/17/15 Pct Recovery = 69% Analysis Date = 02/12/15 Pct Recovery = 69% Analysis Date = 02/12/15 Pct Recovery = 69% Analysis Date = 02/07/15 Pct Recovery = 69% Analysis Date = 02/07/15 Pct Recovery = 69% Analysis Date = 02/02/15 Pct Recovery = 69% Analysis Date = 02/02/15 Pct Recovery = 69% Analysis Date = 01/28/15 Pct Recovery = 69% Analysis Date = 01/28/15 Pct Recovery = 69% Analysis Date = 01/23/15 Pct Recovery = 68% Analysis Date = 01/23/15 Pct Recovery = 68% Analysis Date = 01/18/15 Pct Recovery = 68% Analysis Date = 01/18/15 Pct Recovery = 68% Analysis Date = 01/13/15 Pct Recovery = 68% Analysis Date = 01/13/15 Pct Recovery = 68% Analysis Date = 01/08/15 Pct Recovery = 68% Analysis Date = 01/08/15 Pct Recovery = 68% Analysis Date = 01/03/15 Pct Recovery = 68% Analysis Date = 01/03/15 Pct Recovery = 68% Analysis Date = 12/29/14 Pct Recovery = 68% Analysis Date = 12/29/14 Pct Recovery = 68% Analysis Date = 12/24/14 Pct Recovery = 68% Analysis Date = 12/24/14 Pct Recovery = 68% Analysis Date = 12/19/14 Pct Recovery = 68% Analysis Date = 12/19/14 Pct Recovery = 68% Analysis Date = 12/14/14 Pct Recovery = 68% Analysis Date = 12/14/14 Pct Recovery = 68% Analysis Date = 12/09/14 Pct Recovery = 68% Analysis Date = 12/09/14 Pct Recovery = 68% Analysis Date = 12/04/14 Pct Recovery = 68% Analysis Date = 12/04/14 Pct Recovery = 68% Analysis Date = 11/29/14 Pct Recovery = 67% Analysis Date = 11/29/14 Pct Recovery = 67% Analysis Date = 11/24/14 Pct Recovery = 67% Analysis Date = 11/24/14 Pct Recovery = 67% Analysis Date = 11/19/14 Pct Recovery = 67% Analysis Date = 11/19/14 Pct Recovery = 67% Analysis Date = 11/14/14 Pct Recovery = 67% Analysis Date = 11/14/14 Pct Recovery = 67% Analysis Date = 11/09/14 Pct Recovery = 67% Analysis Date = 11/09/14 Pct Recovery = 67% Analysis Date = 11/04/14 Pct Recovery = 67% Analysis Date = 11/04/14 Pct Recovery = 67% Analysis Date = 10/30/14 Pct Recovery = 67% Analysis Date = 10/30/14 Pct Recovery = 67% Analysis Date = 10/25/14 Pct Recovery = 67% Analysis Date = 10/25/14 Pct Recovery = 67% Analysis Date = 10/20/14 Pct Recovery = 67% Analysis Date = 10/20/14 Pct Recovery = 67% Analysis Date = 10/15/14 Pct Recovery = 67% Analysis Date = 10/15/14 Pct Recovery = 67% Analysis Date = 10/10/14 Pct Recovery = 66% Analysis Date = 10/10/14 Pct Recovery = 66% Analysis Date = 10/05/14 Pct Recovery = 66% Analysis Date = 10/05/14 Pct Recovery = 66% Analysis Date = 09/30/14 Pct Recovery = 66% Analysis Date = 09/30/14 Pct Recovery = 66% Analysis Date = 09/25/14 Pct Recovery = 66% Analysis Date = 09/25/14 Pct Recovery = 66% Analysis Date = 09/20/14 Pct Recovery = 66% Analysis Date = 09/20/14 Pct Recovery = 66% Analysis Date = 09/15/14 Pct Recovery = 66% Analysis Date = 09/15/14 Pct Recovery = 66% Analysis Date = 09/10/14 Pct Recovery = 66% Analysis Date = 09/10/14 Pct Recovery = 66% Analysis Date = 09/05/14 Pct Recovery = 66% Analysis Date = 09/05/14 Pct Recovery = 66% Analysis Date = 08/31/14 Pct Recovery = 66% Analysis Date = 08/31/14 Pct Recovery = 66% Analysis Date = 08/26/14 Pct Recovery = 66% Analysis Date = 08/26/14 Pct Recovery = 66% Analysis Date = 08/21/14 Pct Recovery = 65% Analysis Date = 08/21/14 Pct Recovery = 65% Analysis Date = 08/16/14 Pct Recovery = 65% Analysis Date = 08/16/14 Pct Recovery = 65% Analysis Date = 08/11/14 Pct Recovery = 65% Analysis Date = 08/11/14 Pct Recovery = 65% Analysis Date = 08/06/14 Pct Recovery = 65% Analysis Date = 08/06/14 Pct Recovery = 65% Analysis Date = 08/01/14 Pct Recovery = 65% Analysis Date = 08/01/14 Pct Recovery = 65% Analysis Date = 07/27/14 Pct Recovery = 65% Analysis Date = 07/27/14 Pct Recovery = 65% Analysis Date = 07/22/14 Pct Recovery = 65% Analysis Date = 07/22/14 Pct Recovery = 65% Analysis Date = 07/17/14 Pct Recovery = 65% Analysis Date = 07/17/14 Pct Recovery = 65% Analysis Date = 07/12/14 Pct Recovery = 64% Analysis Date = 07/12/14 Pct Recovery = 64% Analysis Date = 07/07/14 Pct Recovery = 64% Analysis Date = 07/07/14 Pct Recovery = 64% Analysis Date = 07/02/14 Pct Recovery = 64% Analysis Date = 07/02/14 Pct Recovery = 64% Analysis Date = 06/27/14 Pct Recovery = 64% Analysis Date = 06/27/14 Pct Recovery = 64% Analysis Date = 06/22/14 Pct Recovery = 64% Analysis Date = 06/22/14 Pct Recovery = 64% Analysis Date = 06/17/14 Pct Recovery = 64% Analysis Date = 06/17/14 Pct Recovery = 64% Analysis Date = 06/12/14 Pct Recovery = 64% Analysis Date = 06/12/14 Pct Recovery = 64% Analysis Date = 06/07/14 Pct Recovery = 64% Analysis Date = 06/07/14 Pct Recovery = 64% Analysis Date = 06/02/14 Pct Recovery = 63% Analysis Date = 06/02/14 Pct Recovery = 63% Analysis Date = 05/28/14 Pct Recovery = 63% Analysis Date = 05/28/14 Pct Recovery = 63% Analysis Date = 05/23/14 Pct Recovery = 63% Analysis Date = 05/23/14 Pct Recovery = 63% Analysis Date = 05/18/14 Pct Recovery = 63% Analysis Date = 05/18/14 Pct Recovery = 63% Analysis Date = 05/13/14 Pct Recovery = 63% Analysis Date = 05/13/14 Pct Recovery = 63% Analysis Date = 05/08/14 Pct Recovery = 63% Analysis Date = 05/08/14 Pct Recovery = 63% Analysis Date = 05/03/14 Pct Recovery = 63% Analysis Date = 05/03/14 Pct Recovery = 63% Analysis Date = 04/28/14 Pct Recovery = 63% Analysis Date = 04/28/14 Pct Recovery = 63% Analysis Date = 04/23/14 Pct Recovery = 62% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
GLYBURIDE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 10 70% 8% 69% 5%
>= Reporting Level 60 67% 19% 70% 15%
Total 70 68% 17% 69% 13%

Sample Statistics
GLYBURIDE

Characteristic N % % Basis
Plotted 70 92% Spiked
Estimated Values 15 20% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 2 3% Spiked
Spiked 76 .  
False Negatives 4 5% 4 out of 76
Not Spiked 39 .  
False Positives 0 0% 0 out of 39

BQS OBSP Determination:
GUANYLUREA
METHOD: 2440 , TESTIDCODE: 52816LCM56
Open Data Set

The SGPlot Procedure

Sample Statistics
GUANYLUREA

Characteristic N % % Basis
Plotted 0 . Spiked
Estimated Values 0 . Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 . Spiked
Spiked 0 .  
False Negatives 0 . 0 out of 0
Not Spiked 4 .  
False Positives 0 0% 0 out of 4

BQS OBSP Determination:
HEXAMETHYLENETETRAMINE
METHOD: 2440 , TESTIDCODE: 52815LCM56
Open Data Set

The SGPlot Procedure

Sample Statistics
HEXAMETHYLENETETRAMINE

Characteristic N % % Basis
Plotted 0 . Spiked
Estimated Values 0 . Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 . Spiked
Spiked 0 .  
False Negatives 0 . 0 out of 0
Not Spiked 4 .  
False Positives 3 75% 3 out of 4

BQS OBSP Determination:
HYDROCODONE
METHOD: 2440 , TESTIDCODE: 67506LCM56
Open Data Set

Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 68% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 66% Analysis Date = 11/05/15 SpikeMix = ERA 0406-15-08: 80 µl & Abs 052215: 80 µl Pct Recovery = 72% Analysis Date = 11/04/15 SpikeMix = Abs 052215: 80 µl & Abs 050115: 80 µl Pct Recovery = 77% Analysis Date = 09/24/16 SpikeMix = Crescent EN160610015: 80 µl & Abs 061416: 80 µl Pct Recovery = 69% Analysis Date = 09/24/16 SpikeMix = Abs 061416: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 65% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 89% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 89% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 87% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 89% Analysis Date = 11/18/16 SpikeMix = ERA 04281604: 80 µl & ERA 04281603: 80 µl Pct Recovery = 75% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & ERA 04281604: 80 µl Pct Recovery = 71% Analysis Date = 05/07/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 91% Analysis Date = 03/11/15 SpikeMix = ERA 0318-14-02: 15 µl & Abs 041714: 15 µl Pct Recovery = 86% Analysis Date = 01/16/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 77% Analysis Date = 12/06/14 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 69% Analysis Date = 08/21/14 SpikeMix = ERA 0318-14-02: 60 µl & Abs 041714: 60 µl Pct Recovery = 42% Analysis Date = 07/12/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 44% Analysis Date = 06/11/14 SpikeMix = Abs 041614: 60 µl & Abs 041714: 60 µl Pct Recovery = 90% Analysis Date = 05/21/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 74% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-08: 40 µl & Abs 052215: 40 µl Pct Recovery = 84% Analysis Date = 02/23/16 SpikeMix = Abs 052215: 40 µl & Abs 050115: 40 µl Pct Recovery = 69% Analysis Date = 09/10/15 SpikeMix = Abs 052215: 40 µl & ERA 0406-15-07A: 40 µl Pct Recovery = 80% Analysis Date = 07/31/15 SpikeMix = Abs 051315: 40 µl & Abs 052215: 40 µl Pct Recovery = 96% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 110% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 107% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 72% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 69% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 78% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 131% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 103% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 90% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 59% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 65% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 56% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 49% Analysis Date = 11/04/14 SpikeMix = Abs 041714: 8 µl & ERA 0319-14-05: 8 µl Pct Recovery = 43% Analysis Date = 10/10/14 SpikeMix = Abs 041714: 30 µl & Abs 041814: 30 µl Pct Recovery = 117% Analysis Date = 06/28/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 66% Analysis Date = 05/17/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 77% Analysis Date = 02/23/16 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 53% Analysis Date = 11/24/15 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 70% Analysis Date = 08/27/15 SpikeMix = Abs 052215: 20 µl & Abs 050115: 20 µl Pct Recovery = 79% Analysis Date = 07/09/15 SpikeMix = Abs 050115: 20 µl & Abs 052215: 20 µl Pct Recovery = 86% Analysis Date = 12/16/16 Pct Recovery = 78% Analysis Date = 12/11/16 Pct Recovery = 78% Analysis Date = 12/11/16 Pct Recovery = 78% Analysis Date = 12/06/16 Pct Recovery = 78% Analysis Date = 12/06/16 Pct Recovery = 78% Analysis Date = 12/01/16 Pct Recovery = 78% Analysis Date = 12/01/16 Pct Recovery = 78% Analysis Date = 11/27/16 Pct Recovery = 78% Analysis Date = 11/27/16 Pct Recovery = 78% Analysis Date = 11/22/16 Pct Recovery = 78% Analysis Date = 11/22/16 Pct Recovery = 78% Analysis Date = 11/17/16 Pct Recovery = 78% Analysis Date = 11/17/16 Pct Recovery = 78% Analysis Date = 11/12/16 Pct Recovery = 79% Analysis Date = 11/12/16 Pct Recovery = 79% Analysis Date = 11/08/16 Pct Recovery = 79% Analysis Date = 11/08/16 Pct Recovery = 79% Analysis Date = 11/03/16 Pct Recovery = 79% Analysis Date = 11/03/16 Pct Recovery = 79% Analysis Date = 10/29/16 Pct Recovery = 79% Analysis Date = 10/29/16 Pct Recovery = 79% Analysis Date = 10/25/16 Pct Recovery = 79% Analysis Date = 10/25/16 Pct Recovery = 79% Analysis Date = 10/20/16 Pct Recovery = 79% Analysis Date = 10/20/16 Pct Recovery = 79% Analysis Date = 10/15/16 Pct Recovery = 79% Analysis Date = 10/15/16 Pct Recovery = 79% Analysis Date = 10/10/16 Pct Recovery = 79% Analysis Date = 10/10/16 Pct Recovery = 79% Analysis Date = 10/06/16 Pct Recovery = 79% Analysis Date = 10/06/16 Pct Recovery = 79% Analysis Date = 10/01/16 Pct Recovery = 79% Analysis Date = 10/01/16 Pct Recovery = 79% Analysis Date = 09/26/16 Pct Recovery = 79% Analysis Date = 09/26/16 Pct Recovery = 79% Analysis Date = 09/22/16 Pct Recovery = 79% Analysis Date = 09/22/16 Pct Recovery = 79% Analysis Date = 09/17/16 Pct Recovery = 79% Analysis Date = 09/17/16 Pct Recovery = 79% Analysis Date = 09/12/16 Pct Recovery = 79% Analysis Date = 09/12/16 Pct Recovery = 79% Analysis Date = 09/07/16 Pct Recovery = 79% Analysis Date = 09/07/16 Pct Recovery = 79% Analysis Date = 09/03/16 Pct Recovery = 79% Analysis Date = 09/03/16 Pct Recovery = 79% Analysis Date = 08/29/16 Pct Recovery = 79% Analysis Date = 08/29/16 Pct Recovery = 79% Analysis Date = 08/24/16 Pct Recovery = 79% Analysis Date = 08/24/16 Pct Recovery = 79% Analysis Date = 08/20/16 Pct Recovery = 79% Analysis Date = 08/20/16 Pct Recovery = 79% Analysis Date = 08/15/16 Pct Recovery = 79% Analysis Date = 08/15/16 Pct Recovery = 79% Analysis Date = 08/10/16 Pct Recovery = 79% Analysis Date = 08/10/16 Pct Recovery = 79% Analysis Date = 08/05/16 Pct Recovery = 80% Analysis Date = 08/05/16 Pct Recovery = 80% Analysis Date = 08/01/16 Pct Recovery = 80% Analysis Date = 08/01/16 Pct Recovery = 80% Analysis Date = 07/27/16 Pct Recovery = 80% Analysis Date = 07/27/16 Pct Recovery = 80% Analysis Date = 07/22/16 Pct Recovery = 80% Analysis Date = 07/22/16 Pct Recovery = 80% Analysis Date = 07/17/16 Pct Recovery = 80% Analysis Date = 07/17/16 Pct Recovery = 80% Analysis Date = 07/13/16 Pct Recovery = 79% Analysis Date = 07/13/16 Pct Recovery = 79% Analysis Date = 07/08/16 Pct Recovery = 79% Analysis Date = 07/08/16 Pct Recovery = 79% Analysis Date = 07/03/16 Pct Recovery = 79% Analysis Date = 07/03/16 Pct Recovery = 79% Analysis Date = 06/29/16 Pct Recovery = 79% Analysis Date = 06/29/16 Pct Recovery = 79% Analysis Date = 06/24/16 Pct Recovery = 79% Analysis Date = 06/24/16 Pct Recovery = 79% Analysis Date = 06/19/16 Pct Recovery = 79% Analysis Date = 06/19/16 Pct Recovery = 79% Analysis Date = 06/14/16 Pct Recovery = 79% Analysis Date = 06/14/16 Pct Recovery = 79% Analysis Date = 06/10/16 Pct Recovery = 79% Analysis Date = 06/10/16 Pct Recovery = 79% Analysis Date = 06/05/16 Pct Recovery = 79% Analysis Date = 06/05/16 Pct Recovery = 79% Analysis Date = 05/31/16 Pct Recovery = 79% Analysis Date = 05/31/16 Pct Recovery = 79% Analysis Date = 05/27/16 Pct Recovery = 78% Analysis Date = 05/27/16 Pct Recovery = 78% Analysis Date = 05/22/16 Pct Recovery = 78% Analysis Date = 05/22/16 Pct Recovery = 78% Analysis Date = 05/17/16 Pct Recovery = 78% Analysis Date = 05/17/16 Pct Recovery = 78% Analysis Date = 05/12/16 Pct Recovery = 78% Analysis Date = 05/12/16 Pct Recovery = 78% Analysis Date = 05/08/16 Pct Recovery = 78% Analysis Date = 05/08/16 Pct Recovery = 78% Analysis Date = 05/03/16 Pct Recovery = 78% Analysis Date = 05/03/16 Pct Recovery = 78% Analysis Date = 04/28/16 Pct Recovery = 78% Analysis Date = 04/28/16 Pct Recovery = 78% Analysis Date = 04/24/16 Pct Recovery = 78% Analysis Date = 04/24/16 Pct Recovery = 78% Analysis Date = 04/19/16 Pct Recovery = 78% Analysis Date = 04/19/16 Pct Recovery = 78% Analysis Date = 04/14/16 Pct Recovery = 78% Analysis Date = 04/14/16 Pct Recovery = 78% Analysis Date = 04/09/16 Pct Recovery = 77% Analysis Date = 04/09/16 Pct Recovery = 77% Analysis Date = 04/05/16 Pct Recovery = 77% Analysis Date = 04/05/16 Pct Recovery = 77% Analysis Date = 03/31/16 Pct Recovery = 77% Analysis Date = 03/31/16 Pct Recovery = 77% Analysis Date = 03/26/16 Pct Recovery = 77% Analysis Date = 03/26/16 Pct Recovery = 77% Analysis Date = 03/21/16 Pct Recovery = 77% Analysis Date = 03/21/16 Pct Recovery = 77% Analysis Date = 03/17/16 Pct Recovery = 77% Analysis Date = 03/17/16 Pct Recovery = 77% Analysis Date = 03/12/16 Pct Recovery = 77% Analysis Date = 03/12/16 Pct Recovery = 77% Analysis Date = 03/07/16 Pct Recovery = 77% Analysis Date = 03/07/16 Pct Recovery = 77% Analysis Date = 03/03/16 Pct Recovery = 77% Analysis Date = 03/03/16 Pct Recovery = 77% Analysis Date = 02/27/16 Pct Recovery = 77% Analysis Date = 02/27/16 Pct Recovery = 77% Analysis Date = 02/22/16 Pct Recovery = 77% Analysis Date = 02/22/16 Pct Recovery = 77% Analysis Date = 02/17/16 Pct Recovery = 77% Analysis Date = 02/17/16 Pct Recovery = 77% Analysis Date = 02/13/16 Pct Recovery = 77% Analysis Date = 02/13/16 Pct Recovery = 77% Analysis Date = 02/08/16 Pct Recovery = 77% Analysis Date = 02/08/16 Pct Recovery = 77% Analysis Date = 02/03/16 Pct Recovery = 77% Analysis Date = 02/03/16 Pct Recovery = 77% Analysis Date = 01/30/16 Pct Recovery = 77% Analysis Date = 01/30/16 Pct Recovery = 77% Analysis Date = 01/25/16 Pct Recovery = 77% Analysis Date = 01/25/16 Pct Recovery = 77% Analysis Date = 01/20/16 Pct Recovery = 77% Analysis Date = 01/20/16 Pct Recovery = 77% Analysis Date = 01/15/16 Pct Recovery = 77% Analysis Date = 01/15/16 Pct Recovery = 77% Analysis Date = 01/11/16 Pct Recovery = 77% Analysis Date = 01/11/16 Pct Recovery = 77% Analysis Date = 01/06/16 Pct Recovery = 77% Analysis Date = 01/06/16 Pct Recovery = 77% Analysis Date = 01/01/16 Pct Recovery = 77% Analysis Date = 01/01/16 Pct Recovery = 77% Analysis Date = 12/28/15 Pct Recovery = 77% Analysis Date = 12/28/15 Pct Recovery = 77% Analysis Date = 12/23/15 Pct Recovery = 78% Analysis Date = 12/23/15 Pct Recovery = 78% Analysis Date = 12/18/15 Pct Recovery = 78% Analysis Date = 12/18/15 Pct Recovery = 78% Analysis Date = 12/13/15 Pct Recovery = 78% Analysis Date = 12/13/15 Pct Recovery = 78% Analysis Date = 12/09/15 Pct Recovery = 78% Analysis Date = 12/09/15 Pct Recovery = 78% Analysis Date = 12/04/15 Pct Recovery = 78% Analysis Date = 12/04/15 Pct Recovery = 78% Analysis Date = 11/29/15 Pct Recovery = 78% Analysis Date = 11/29/15 Pct Recovery = 78% Analysis Date = 11/24/15 Pct Recovery = 78% Analysis Date = 11/24/15 Pct Recovery = 78% Analysis Date = 11/20/15 Pct Recovery = 78% Analysis Date = 11/20/15 Pct Recovery = 78% Analysis Date = 11/15/15 Pct Recovery = 78% Analysis Date = 11/15/15 Pct Recovery = 78% Analysis Date = 11/10/15 Pct Recovery = 78% Analysis Date = 11/10/15 Pct Recovery = 78% Analysis Date = 11/06/15 Pct Recovery = 78% Analysis Date = 11/06/15 Pct Recovery = 78% Analysis Date = 11/01/15 Pct Recovery = 78% Analysis Date = 11/01/15 Pct Recovery = 78% Analysis Date = 10/27/15 Pct Recovery = 78% Analysis Date = 10/27/15 Pct Recovery = 78% Analysis Date = 10/22/15 Pct Recovery = 78% Analysis Date = 10/22/15 Pct Recovery = 78% Analysis Date = 10/18/15 Pct Recovery = 78% Analysis Date = 10/18/15 Pct Recovery = 78% Analysis Date = 10/13/15 Pct Recovery = 78% Analysis Date = 10/13/15 Pct Recovery = 78% Analysis Date = 10/08/15 Pct Recovery = 78% Analysis Date = 10/08/15 Pct Recovery = 78% Analysis Date = 10/04/15 Pct Recovery = 78% Analysis Date = 10/04/15 Pct Recovery = 78% Analysis Date = 09/29/15 Pct Recovery = 78% Analysis Date = 09/29/15 Pct Recovery = 78% Analysis Date = 09/24/15 Pct Recovery = 79% Analysis Date = 09/24/15 Pct Recovery = 79% Analysis Date = 09/19/15 Pct Recovery = 79% Analysis Date = 09/19/15 Pct Recovery = 79% Analysis Date = 09/15/15 Pct Recovery = 79% Analysis Date = 09/15/15 Pct Recovery = 79% Analysis Date = 09/10/15 Pct Recovery = 79% Analysis Date = 09/10/15 Pct Recovery = 79% Analysis Date = 09/05/15 Pct Recovery = 79% Analysis Date = 09/05/15 Pct Recovery = 79% Analysis Date = 09/01/15 Pct Recovery = 79% Analysis Date = 09/01/15 Pct Recovery = 79% Analysis Date = 08/27/15 Pct Recovery = 79% Analysis Date = 08/27/15 Pct Recovery = 79% Analysis Date = 08/22/15 Pct Recovery = 79% Analysis Date = 08/22/15 Pct Recovery = 79% Analysis Date = 08/17/15 Pct Recovery = 79% Analysis Date = 08/17/15 Pct Recovery = 79% Analysis Date = 08/13/15 Pct Recovery = 79% Analysis Date = 08/13/15 Pct Recovery = 79% Analysis Date = 08/08/15 Pct Recovery = 79% Analysis Date = 08/08/15 Pct Recovery = 79% Analysis Date = 08/03/15 Pct Recovery = 79% Analysis Date = 08/03/15 Pct Recovery = 79% Analysis Date = 07/29/15 Pct Recovery = 79% Analysis Date = 07/29/15 Pct Recovery = 79% Analysis Date = 07/25/15 Pct Recovery = 79% Analysis Date = 07/25/15 Pct Recovery = 79% Analysis Date = 07/20/15 Pct Recovery = 79% Analysis Date = 07/20/15 Pct Recovery = 79% Analysis Date = 07/15/15 Pct Recovery = 79% Analysis Date = 07/15/15 Pct Recovery = 79% Analysis Date = 07/11/15 Pct Recovery = 79% Analysis Date = 07/11/15 Pct Recovery = 79% Analysis Date = 07/06/15 Pct Recovery = 78% Analysis Date = 07/06/15 Pct Recovery = 78% Analysis Date = 07/01/15 Pct Recovery = 78% Analysis Date = 07/01/15 Pct Recovery = 78% Analysis Date = 06/26/15 Pct Recovery = 78% Analysis Date = 06/26/15 Pct Recovery = 78% Analysis Date = 06/22/15 Pct Recovery = 78% Analysis Date = 06/22/15 Pct Recovery = 78% Analysis Date = 06/17/15 Pct Recovery = 78% Analysis Date = 06/17/15 Pct Recovery = 78% Analysis Date = 06/12/15 Pct Recovery = 78% Analysis Date = 06/12/15 Pct Recovery = 78% Analysis Date = 06/08/15 Pct Recovery = 78% Analysis Date = 06/08/15 Pct Recovery = 78% Analysis Date = 06/03/15 Pct Recovery = 78% Analysis Date = 06/03/15 Pct Recovery = 78% Analysis Date = 05/29/15 Pct Recovery = 78% Analysis Date = 05/29/15 Pct Recovery = 78% Analysis Date = 05/24/15 Pct Recovery = 77% Analysis Date = 05/24/15 Pct Recovery = 77% Analysis Date = 05/20/15 Pct Recovery = 77% Analysis Date = 05/20/15 Pct Recovery = 77% Analysis Date = 05/15/15 Pct Recovery = 77% Analysis Date = 05/15/15 Pct Recovery = 77% Analysis Date = 05/10/15 Pct Recovery = 77% Analysis Date = 05/10/15 Pct Recovery = 77% Analysis Date = 05/06/15 Pct Recovery = 77% Analysis Date = 05/06/15 Pct Recovery = 77% Analysis Date = 05/01/15 Pct Recovery = 77% Analysis Date = 05/01/15 Pct Recovery = 77% Analysis Date = 04/26/15 Pct Recovery = 77% Analysis Date = 04/26/15 Pct Recovery = 77% Analysis Date = 04/21/15 Pct Recovery = 77% Analysis Date = 04/21/15 Pct Recovery = 77% Analysis Date = 04/17/15 Pct Recovery = 77% Analysis Date = 04/17/15 Pct Recovery = 77% Analysis Date = 04/12/15 Pct Recovery = 77% Analysis Date = 04/12/15 Pct Recovery = 77% Analysis Date = 04/07/15 Pct Recovery = 76% Analysis Date = 04/07/15 Pct Recovery = 76% Analysis Date = 04/02/15 Pct Recovery = 76% Analysis Date = 04/02/15 Pct Recovery = 76% Analysis Date = 03/29/15 Pct Recovery = 76% Analysis Date = 03/29/15 Pct Recovery = 76% Analysis Date = 03/24/15 Pct Recovery = 76% Analysis Date = 03/24/15 Pct Recovery = 76% Analysis Date = 03/19/15 Pct Recovery = 76% Analysis Date = 03/19/15 Pct Recovery = 76% Analysis Date = 03/15/15 Pct Recovery = 76% Analysis Date = 03/15/15 Pct Recovery = 76% Analysis Date = 03/10/15 Pct Recovery = 76% Analysis Date = 03/10/15 Pct Recovery = 76% Analysis Date = 03/05/15 Pct Recovery = 76% Analysis Date = 03/05/15 Pct Recovery = 76% Analysis Date = 02/28/15 Pct Recovery = 76% Analysis Date = 02/28/15 Pct Recovery = 76% Analysis Date = 02/24/15 Pct Recovery = 76% Analysis Date = 02/24/15 Pct Recovery = 76% Analysis Date = 02/19/15 Pct Recovery = 75% Analysis Date = 02/19/15 Pct Recovery = 75% Analysis Date = 02/14/15 Pct Recovery = 75% Analysis Date = 02/14/15 Pct Recovery = 75% Analysis Date = 02/10/15 Pct Recovery = 75% Analysis Date = 02/10/15 Pct Recovery = 75% Analysis Date = 02/05/15 Pct Recovery = 75% Analysis Date = 02/05/15 Pct Recovery = 75% Analysis Date = 01/31/15 Pct Recovery = 75% Analysis Date = 01/31/15 Pct Recovery = 75% Analysis Date = 01/26/15 Pct Recovery = 75% Analysis Date = 01/26/15 Pct Recovery = 75% Analysis Date = 01/22/15 Pct Recovery = 75% Analysis Date = 01/22/15 Pct Recovery = 75% Analysis Date = 01/17/15 Pct Recovery = 75% Analysis Date = 01/17/15 Pct Recovery = 75% Analysis Date = 01/12/15 Pct Recovery = 75% Analysis Date = 01/12/15 Pct Recovery = 75% Analysis Date = 01/08/15 Pct Recovery = 75% Analysis Date = 01/08/15 Pct Recovery = 75% Analysis Date = 01/03/15 Pct Recovery = 74% Analysis Date = 01/03/15 Pct Recovery = 74% Analysis Date = 12/29/14 Pct Recovery = 74% Analysis Date = 12/29/14 Pct Recovery = 74% Analysis Date = 12/24/14 Pct Recovery = 74% Analysis Date = 12/24/14 Pct Recovery = 74% Analysis Date = 12/20/14 Pct Recovery = 74% Analysis Date = 12/20/14 Pct Recovery = 74% Analysis Date = 12/15/14 Pct Recovery = 74% Analysis Date = 12/15/14 Pct Recovery = 74% Analysis Date = 12/10/14 Pct Recovery = 74% Analysis Date = 12/10/14 Pct Recovery = 74% Analysis Date = 12/05/14 Pct Recovery = 74% Analysis Date = 12/05/14 Pct Recovery = 74% Analysis Date = 12/01/14 Pct Recovery = 74% Analysis Date = 12/01/14 Pct Recovery = 74% Analysis Date = 11/26/14 Pct Recovery = 74% Analysis Date = 11/26/14 Pct Recovery = 74% Analysis Date = 11/21/14 Pct Recovery = 74% Analysis Date = 11/21/14 Pct Recovery = 74% Analysis Date = 11/17/14 Pct Recovery = 74% Analysis Date = 11/17/14 Pct Recovery = 74% Analysis Date = 11/12/14 Pct Recovery = 73% Analysis Date = 11/12/14 Pct Recovery = 73% Analysis Date = 11/07/14 Pct Recovery = 73% Analysis Date = 11/07/14 Pct Recovery = 73% Analysis Date = 11/02/14 Pct Recovery = 73% Analysis Date = 11/02/14 Pct Recovery = 73% Analysis Date = 10/29/14 Pct Recovery = 73% Analysis Date = 10/29/14 Pct Recovery = 73% Analysis Date = 10/24/14 Pct Recovery = 73% Analysis Date = 10/24/14 Pct Recovery = 73% Analysis Date = 10/19/14 Pct Recovery = 73% Analysis Date = 10/19/14 Pct Recovery = 73% Analysis Date = 10/15/14 Pct Recovery = 73% Analysis Date = 10/15/14 Pct Recovery = 73% Analysis Date = 10/10/14 Pct Recovery = 73% Analysis Date = 10/10/14 Pct Recovery = 73% Analysis Date = 10/05/14 Pct Recovery = 73% Analysis Date = 10/05/14 Pct Recovery = 73% Analysis Date = 09/30/14 Pct Recovery = 73% Analysis Date = 09/30/14 Pct Recovery = 73% Analysis Date = 09/26/14 Pct Recovery = 72% Analysis Date = 09/26/14 Pct Recovery = 72% Analysis Date = 09/21/14 Pct Recovery = 72% Analysis Date = 09/21/14 Pct Recovery = 72% Analysis Date = 09/16/14 Pct Recovery = 72% Analysis Date = 09/16/14 Pct Recovery = 72% Analysis Date = 09/12/14 Pct Recovery = 72% Analysis Date = 09/12/14 Pct Recovery = 72% Analysis Date = 09/07/14 Pct Recovery = 72% Analysis Date = 09/07/14 Pct Recovery = 72% Analysis Date = 09/02/14 Pct Recovery = 72% Analysis Date = 09/02/14 Pct Recovery = 72% Analysis Date = 08/28/14 Pct Recovery = 72% Analysis Date = 08/28/14 Pct Recovery = 72% Analysis Date = 08/24/14 Pct Recovery = 72% Analysis Date = 08/24/14 Pct Recovery = 72% Analysis Date = 08/19/14 Pct Recovery = 72% Analysis Date = 08/19/14 Pct Recovery = 72% Analysis Date = 08/14/14 Pct Recovery = 72% Analysis Date = 08/14/14 Pct Recovery = 72% Analysis Date = 08/09/14 Pct Recovery = 71% Analysis Date = 08/09/14 Pct Recovery = 71% Analysis Date = 08/05/14 Pct Recovery = 71% Analysis Date = 08/05/14 Pct Recovery = 71% Analysis Date = 07/31/14 Pct Recovery = 71% Analysis Date = 07/31/14 Pct Recovery = 71% Analysis Date = 07/26/14 Pct Recovery = 71% Analysis Date = 07/26/14 Pct Recovery = 71% Analysis Date = 07/22/14 Pct Recovery = 71% Analysis Date = 07/22/14 Pct Recovery = 71% Analysis Date = 07/17/14 Pct Recovery = 71% Analysis Date = 07/17/14 Pct Recovery = 71% Analysis Date = 07/12/14 Pct Recovery = 71% Analysis Date = 07/12/14 Pct Recovery = 71% Analysis Date = 07/07/14 Pct Recovery = 71% Analysis Date = 07/07/14 Pct Recovery = 71% Analysis Date = 07/03/14 Pct Recovery = 71% Analysis Date = 07/03/14 Pct Recovery = 71% Analysis Date = 06/28/14 Pct Recovery = 70% Analysis Date = 06/28/14 Pct Recovery = 70% Analysis Date = 06/23/14 Pct Recovery = 70% Analysis Date = 06/23/14 Pct Recovery = 70% Analysis Date = 06/19/14 Pct Recovery = 70% Analysis Date = 06/19/14 Pct Recovery = 70% Analysis Date = 06/14/14 Pct Recovery = 70% Analysis Date = 06/14/14 Pct Recovery = 70% Analysis Date = 06/09/14 Pct Recovery = 70% Analysis Date = 06/09/14 Pct Recovery = 70% Analysis Date = 06/04/14 Pct Recovery = 70% Analysis Date = 06/04/14 Pct Recovery = 70% Analysis Date = 05/31/14 Pct Recovery = 70% Analysis Date = 05/31/14 Pct Recovery = 70% Analysis Date = 05/26/14 Pct Recovery = 70% Analysis Date = 05/26/14 Pct Recovery = 70% Analysis Date = 05/21/14 Pct Recovery = 69% Analysis Date = 05/21/14 Pct Recovery = 69% Analysis Date = 05/17/14 Pct Recovery = 69% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
HYDROCODONE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 44 77% 19% 76% 16%
Total 44 77% 19% 76% 16%

Sample Statistics
HYDROCODONE

Characteristic N % % Basis
Plotted 44 86% Spiked
Estimated Values 17 33% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 4 8% Spiked
Spiked 51 .  
False Negatives 3 6% 3 out of 51
Not Spiked 64 .  
False Positives 0 0% 0 out of 64

BQS OBSP Determination:
HYDROCORTISONE
METHOD: 2440 , TESTIDCODE: 67459LCM56
Open Data Set

Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 76% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 79% Analysis Date = 11/05/15 SpikeMix = ERA 0406-15-08: 80 µl & Abs 052215: 80 µl Pct Recovery = 82% Analysis Date = 11/04/15 SpikeMix = Abs 052215: 80 µl & Abs 050115: 80 µl Pct Recovery = 88% Analysis Date = 01/17/16 SpikeMix = ERA 0406-15-09: 80 µl & ERA 0406-15-07A: 80 µl Pct Recovery = 74% Analysis Date = 11/24/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 89% Analysis Date = 09/24/16 SpikeMix = Crescent EN160610015: 80 µl & Abs 061416: 80 µl Pct Recovery = 75% Analysis Date = 09/24/16 SpikeMix = Abs 061416: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 75% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 91% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 87% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 86% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 84% Analysis Date = 11/18/16 SpikeMix = ERA 04281604: 80 µl & ERA 04281603: 80 µl Pct Recovery = 70% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & ERA 04281604: 80 µl Pct Recovery = 68% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 80% Analysis Date = 12/07/14 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 76% Analysis Date = 10/25/14 SpikeMix = Abs 041614: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 78% Analysis Date = 06/22/14 SpikeMix = Abs 041814: 60 µl & Abs 041614: 60 µl Pct Recovery = 120% Analysis Date = 06/11/14 SpikeMix = Abs 041614: 60 µl & Abs 041714: 60 µl Pct Recovery = 99% Analysis Date = 04/29/15 SpikeMix = ERA 0319-14-05: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 103% Analysis Date = 03/11/15 SpikeMix = ERA 0318-14-02: 15 µl & Abs 041714: 15 µl Pct Recovery = 93% Analysis Date = 02/06/15 SpikeMix = Abs 041814: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 89% Analysis Date = 12/06/14 SpikeMix = ERA 0318-14-02: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 77% Analysis Date = 10/11/14 SpikeMix = ERA 0318-14-02: 60 µl & ERA 0319-14-04: 60 µl Pct Recovery = 82% Analysis Date = 08/21/14 SpikeMix = ERA 0318-14-02: 60 µl & Abs 041714: 60 µl Pct Recovery = 65% Analysis Date = 07/26/14 SpikeMix = ERA 0319-14-05: 60 µl & ERA 0318-14-02: 60 µl Pct Recovery = 119% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-08: 40 µl & Abs 052215: 40 µl Pct Recovery = 93% Analysis Date = 02/23/16 SpikeMix = Abs 052215: 40 µl & Abs 050115: 40 µl Pct Recovery = 66% Analysis Date = 09/10/15 SpikeMix = Abs 052215: 40 µl & ERA 0406-15-07A: 40 µl Pct Recovery = 85% Analysis Date = 07/31/15 SpikeMix = Abs 051315: 40 µl & Abs 052215: 40 µl Pct Recovery = 87% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-08: 40 µl & ERA 0406-15-09: 40 µl Pct Recovery = 81% Analysis Date = 07/31/15 SpikeMix = ERA 0406-15-09: 40 µl & Abs 050115: 40 µl Pct Recovery = 104% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 75% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 81% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 71% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 72% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 72% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 65% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 81% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 73% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 98% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 98% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 88% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 85% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 75% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 80% Analysis Date = 04/30/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 97% Analysis Date = 02/10/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 76% Analysis Date = 10/24/14 SpikeMix = ERA 0319-14-05: 8 µl & Abs 041614: 8 µl Pct Recovery = 87% Analysis Date = 12/07/14 SpikeMix = ERA 0318-14-02: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 94% Analysis Date = 11/04/14 SpikeMix = Abs 041814: 8 µl & ERA 0318-14-02: 8 µl Pct Recovery = 87% Analysis Date = 09/12/14 SpikeMix = Abs 041614: 30 µl & ERA 0319-14-04: 30 µl Pct Recovery = 58% Analysis Date = 06/28/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 75% Analysis Date = 05/30/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 87% Analysis Date = 05/17/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 83% Analysis Date = 10/10/14 SpikeMix = Abs 041814: 30 µl & ERA 0318-14-02: 30 µl Pct Recovery = 92% Analysis Date = 08/30/14 SpikeMix = ERA 0318-14-02: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 91% Analysis Date = 07/20/14 SpikeMix = ERA 0318-14-02: 30 µl & Abs 041714: 30 µl Pct Recovery = 63% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 75% Analysis Date = 02/23/16 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 82% Analysis Date = 11/24/15 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 85% Analysis Date = 09/09/15 SpikeMix = ERA 0406-15-08: 20 µl & Abs 052215: 20 µl Pct Recovery = 73% Analysis Date = 08/27/15 SpikeMix = Abs 052215: 20 µl & Abs 050115: 20 µl Pct Recovery = 81% Analysis Date = 07/09/15 SpikeMix = Abs 050115: 20 µl & Abs 052215: 20 µl Pct Recovery = 96% Analysis Date = 06/26/15 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 85% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-08: 20 µl & ERA 0406-15-09: 20 µl Pct Recovery = 80% Analysis Date = 11/24/15 SpikeMix = ERA 0406-15-09: 20 µl & Abs 050115: 20 µl Pct Recovery = 93% Analysis Date = 01/04/17 Pct Recovery = 80% Analysis Date = 12/31/16 Pct Recovery = 80% Analysis Date = 12/31/16 Pct Recovery = 80% Analysis Date = 12/26/16 Pct Recovery = 80% Analysis Date = 12/26/16 Pct Recovery = 80% Analysis Date = 12/21/16 Pct Recovery = 80% Analysis Date = 12/21/16 Pct Recovery = 80% Analysis Date = 12/16/16 Pct Recovery = 80% Analysis Date = 12/16/16 Pct Recovery = 80% Analysis Date = 12/11/16 Pct Recovery = 80% Analysis Date = 12/11/16 Pct Recovery = 80% Analysis Date = 12/07/16 Pct Recovery = 80% Analysis Date = 12/07/16 Pct Recovery = 80% Analysis Date = 12/02/16 Pct Recovery = 80% Analysis Date = 12/02/16 Pct Recovery = 80% Analysis Date = 11/27/16 Pct Recovery = 80% Analysis Date = 11/27/16 Pct Recovery = 80% Analysis Date = 11/22/16 Pct Recovery = 80% Analysis Date = 11/22/16 Pct Recovery = 80% Analysis Date = 11/17/16 Pct Recovery = 80% Analysis Date = 11/17/16 Pct Recovery = 80% Analysis Date = 11/12/16 Pct Recovery = 80% Analysis Date = 11/12/16 Pct Recovery = 80% Analysis Date = 11/08/16 Pct Recovery = 80% Analysis Date = 11/08/16 Pct Recovery = 80% Analysis Date = 11/03/16 Pct Recovery = 80% Analysis Date = 11/03/16 Pct Recovery = 80% Analysis Date = 10/29/16 Pct Recovery = 80% Analysis Date = 10/29/16 Pct Recovery = 80% Analysis Date = 10/24/16 Pct Recovery = 80% Analysis Date = 10/24/16 Pct Recovery = 80% Analysis Date = 10/19/16 Pct Recovery = 80% Analysis Date = 10/19/16 Pct Recovery = 80% Analysis Date = 10/15/16 Pct Recovery = 80% Analysis Date = 10/15/16 Pct Recovery = 80% Analysis Date = 10/10/16 Pct Recovery = 80% Analysis Date = 10/10/16 Pct Recovery = 80% Analysis Date = 10/05/16 Pct Recovery = 80% Analysis Date = 10/05/16 Pct Recovery = 80% Analysis Date = 09/30/16 Pct Recovery = 80% Analysis Date = 09/30/16 Pct Recovery = 80% Analysis Date = 09/25/16 Pct Recovery = 80% Analysis Date = 09/25/16 Pct Recovery = 80% Analysis Date = 09/20/16 Pct Recovery = 80% Analysis Date = 09/20/16 Pct Recovery = 80% Analysis Date = 09/16/16 Pct Recovery = 79% Analysis Date = 09/16/16 Pct Recovery = 79% Analysis Date = 09/11/16 Pct Recovery = 79% Analysis Date = 09/11/16 Pct Recovery = 79% Analysis Date = 09/06/16 Pct Recovery = 79% Analysis Date = 09/06/16 Pct Recovery = 79% Analysis Date = 09/01/16 Pct Recovery = 79% Analysis Date = 09/01/16 Pct Recovery = 79% Analysis Date = 08/27/16 Pct Recovery = 79% Analysis Date = 08/27/16 Pct Recovery = 79% Analysis Date = 08/23/16 Pct Recovery = 79% Analysis Date = 08/23/16 Pct Recovery = 79% Analysis Date = 08/18/16 Pct Recovery = 79% Analysis Date = 08/18/16 Pct Recovery = 79% Analysis Date = 08/13/16 Pct Recovery = 79% Analysis Date = 08/13/16 Pct Recovery = 79% Analysis Date = 08/08/16 Pct Recovery = 79% Analysis Date = 08/08/16 Pct Recovery = 79% Analysis Date = 08/03/16 Pct Recovery = 79% Analysis Date = 08/03/16 Pct Recovery = 79% Analysis Date = 07/29/16 Pct Recovery = 80% Analysis Date = 07/29/16 Pct Recovery = 80% Analysis Date = 07/25/16 Pct Recovery = 80% Analysis Date = 07/25/16 Pct Recovery = 80% Analysis Date = 07/20/16 Pct Recovery = 80% Analysis Date = 07/20/16 Pct Recovery = 80% Analysis Date = 07/15/16 Pct Recovery = 80% Analysis Date = 07/15/16 Pct Recovery = 80% Analysis Date = 07/10/16 Pct Recovery = 80% Analysis Date = 07/10/16 Pct Recovery = 80% Analysis Date = 07/05/16 Pct Recovery = 80% Analysis Date = 07/05/16 Pct Recovery = 80% Analysis Date = 07/01/16 Pct Recovery = 80% Analysis Date = 07/01/16 Pct Recovery = 80% Analysis Date = 06/26/16 Pct Recovery = 80% Analysis Date = 06/26/16 Pct Recovery = 80% Analysis Date = 06/21/16 Pct Recovery = 80% Analysis Date = 06/21/16 Pct Recovery = 80% Analysis Date = 06/16/16 Pct Recovery = 80% Analysis Date = 06/16/16 Pct Recovery = 80% Analysis Date = 06/11/16 Pct Recovery = 80% Analysis Date = 06/11/16 Pct Recovery = 80% Analysis Date = 06/06/16 Pct Recovery = 80% Analysis Date = 06/06/16 Pct Recovery = 80% Analysis Date = 06/02/16 Pct Recovery = 80% Analysis Date = 06/02/16 Pct Recovery = 80% Analysis Date = 05/28/16 Pct Recovery = 80% Analysis Date = 05/28/16 Pct Recovery = 80% Analysis Date = 05/23/16 Pct Recovery = 80% Analysis Date = 05/23/16 Pct Recovery = 80% Analysis Date = 05/18/16 Pct Recovery = 80% Analysis Date = 05/18/16 Pct Recovery = 80% Analysis Date = 05/13/16 Pct Recovery = 80% Analysis Date = 05/13/16 Pct Recovery = 80% Analysis Date = 05/08/16 Pct Recovery = 80% Analysis Date = 05/08/16 Pct Recovery = 80% Analysis Date = 05/04/16 Pct Recovery = 80% Analysis Date = 05/04/16 Pct Recovery = 80% Analysis Date = 04/29/16 Pct Recovery = 80% Analysis Date = 04/29/16 Pct Recovery = 80% Analysis Date = 04/24/16 Pct Recovery = 80% Analysis Date = 04/24/16 Pct Recovery = 80% Analysis Date = 04/19/16 Pct Recovery = 80% Analysis Date = 04/19/16 Pct Recovery = 80% Analysis Date = 04/14/16 Pct Recovery = 81% Analysis Date = 04/14/16 Pct Recovery = 81% Analysis Date = 04/10/16 Pct Recovery = 81% Analysis Date = 04/10/16 Pct Recovery = 81% Analysis Date = 04/05/16 Pct Recovery = 81% Analysis Date = 04/05/16 Pct Recovery = 81% Analysis Date = 03/31/16 Pct Recovery = 81% Analysis Date = 03/31/16 Pct Recovery = 81% Analysis Date = 03/26/16 Pct Recovery = 81% Analysis Date = 03/26/16 Pct Recovery = 81% Analysis Date = 03/21/16 Pct Recovery = 81% Analysis Date = 03/21/16 Pct Recovery = 81% Analysis Date = 03/16/16 Pct Recovery = 81% Analysis Date = 03/16/16 Pct Recovery = 81% Analysis Date = 03/12/16 Pct Recovery = 81% Analysis Date = 03/12/16 Pct Recovery = 81% Analysis Date = 03/07/16 Pct Recovery = 81% Analysis Date = 03/07/16 Pct Recovery = 81% Analysis Date = 03/02/16 Pct Recovery = 82% Analysis Date = 03/02/16 Pct Recovery = 82% Analysis Date = 02/26/16 Pct Recovery = 82% Analysis Date = 02/26/16 Pct Recovery = 82% Analysis Date = 02/21/16 Pct Recovery = 82% Analysis Date = 02/21/16 Pct Recovery = 82% Analysis Date = 02/17/16 Pct Recovery = 82% Analysis Date = 02/17/16 Pct Recovery = 82% Analysis Date = 02/12/16 Pct Recovery = 82% Analysis Date = 02/12/16 Pct Recovery = 82% Analysis Date = 02/07/16 Pct Recovery = 82% Analysis Date = 02/07/16 Pct Recovery = 82% Analysis Date = 02/02/16 Pct Recovery = 82% Analysis Date = 02/02/16 Pct Recovery = 82% Analysis Date = 01/28/16 Pct Recovery = 82% Analysis Date = 01/28/16 Pct Recovery = 82% Analysis Date = 01/23/16 Pct Recovery = 83% Analysis Date = 01/23/16 Pct Recovery = 83% Analysis Date = 01/19/16 Pct Recovery = 83% Analysis Date = 01/19/16 Pct Recovery = 83% Analysis Date = 01/14/16 Pct Recovery = 83% Analysis Date = 01/14/16 Pct Recovery = 83% Analysis Date = 01/09/16 Pct Recovery = 83% Analysis Date = 01/09/16 Pct Recovery = 83% Analysis Date = 01/04/16 Pct Recovery = 83% Analysis Date = 01/04/16 Pct Recovery = 83% Analysis Date = 12/30/15 Pct Recovery = 83% Analysis Date = 12/30/15 Pct Recovery = 83% Analysis Date = 12/26/15 Pct Recovery = 83% Analysis Date = 12/26/15 Pct Recovery = 83% Analysis Date = 12/21/15 Pct Recovery = 83% Analysis Date = 12/21/15 Pct Recovery = 83% Analysis Date = 12/16/15 Pct Recovery = 84% Analysis Date = 12/16/15 Pct Recovery = 84% Analysis Date = 12/11/15 Pct Recovery = 84% Analysis Date = 12/11/15 Pct Recovery = 84% Analysis Date = 12/06/15 Pct Recovery = 84% Analysis Date = 12/06/15 Pct Recovery = 84% Analysis Date = 12/01/15 Pct Recovery = 84% Analysis Date = 12/01/15 Pct Recovery = 84% Analysis Date = 11/27/15 Pct Recovery = 84% Analysis Date = 11/27/15 Pct Recovery = 84% Analysis Date = 11/22/15 Pct Recovery = 84% Analysis Date = 11/22/15 Pct Recovery = 84% Analysis Date = 11/17/15 Pct Recovery = 84% Analysis Date = 11/17/15 Pct Recovery = 84% Analysis Date = 11/12/15 Pct Recovery = 85% Analysis Date = 11/12/15 Pct Recovery = 85% Analysis Date = 11/07/15 Pct Recovery = 85% Analysis Date = 11/07/15 Pct Recovery = 85% Analysis Date = 11/03/15 Pct Recovery = 85% Analysis Date = 11/03/15 Pct Recovery = 85% Analysis Date = 10/29/15 Pct Recovery = 85% Analysis Date = 10/29/15 Pct Recovery = 85% Analysis Date = 10/24/15 Pct Recovery = 85% Analysis Date = 10/24/15 Pct Recovery = 85% Analysis Date = 10/19/15 Pct Recovery = 85% Analysis Date = 10/19/15 Pct Recovery = 85% Analysis Date = 10/14/15 Pct Recovery = 85% Analysis Date = 10/14/15 Pct Recovery = 85% Analysis Date = 10/09/15 Pct Recovery = 85% Analysis Date = 10/09/15 Pct Recovery = 85% Analysis Date = 10/05/15 Pct Recovery = 85% Analysis Date = 10/05/15 Pct Recovery = 85% Analysis Date = 09/30/15 Pct Recovery = 85% Analysis Date = 09/30/15 Pct Recovery = 85% Analysis Date = 09/25/15 Pct Recovery = 85% Analysis Date = 09/25/15 Pct Recovery = 85% Analysis Date = 09/20/15 Pct Recovery = 85% Analysis Date = 09/20/15 Pct Recovery = 85% Analysis Date = 09/15/15 Pct Recovery = 85% Analysis Date = 09/15/15 Pct Recovery = 85% Analysis Date = 09/10/15 Pct Recovery = 85% Analysis Date = 09/10/15 Pct Recovery = 85% Analysis Date = 09/06/15 Pct Recovery = 85% Analysis Date = 09/06/15 Pct Recovery = 85% Analysis Date = 09/01/15 Pct Recovery = 85% Analysis Date = 09/01/15 Pct Recovery = 85% Analysis Date = 08/27/15 Pct Recovery = 85% Analysis Date = 08/27/15 Pct Recovery = 85% Analysis Date = 08/22/15 Pct Recovery = 85% Analysis Date = 08/22/15 Pct Recovery = 85% Analysis Date = 08/17/15 Pct Recovery = 86% Analysis Date = 08/17/15 Pct Recovery = 86% Analysis Date = 08/13/15 Pct Recovery = 86% Analysis Date = 08/13/15 Pct Recovery = 86% Analysis Date = 08/08/15 Pct Recovery = 86% Analysis Date = 08/08/15 Pct Recovery = 86% Analysis Date = 08/03/15 Pct Recovery = 86% Analysis Date = 08/03/15 Pct Recovery = 86% Analysis Date = 07/29/15 Pct Recovery = 86% Analysis Date = 07/29/15 Pct Recovery = 86% Analysis Date = 07/24/15 Pct Recovery = 86% Analysis Date = 07/24/15 Pct Recovery = 86% Analysis Date = 07/19/15 Pct Recovery = 86% Analysis Date = 07/19/15 Pct Recovery = 86% Analysis Date = 07/15/15 Pct Recovery = 86% Analysis Date = 07/15/15 Pct Recovery = 86% Analysis Date = 07/10/15 Pct Recovery = 86% Analysis Date = 07/10/15 Pct Recovery = 86% Analysis Date = 07/05/15 Pct Recovery = 86% Analysis Date = 07/05/15 Pct Recovery = 86% Analysis Date = 06/30/15 Pct Recovery = 86% Analysis Date = 06/30/15 Pct Recovery = 86% Analysis Date = 06/25/15 Pct Recovery = 86% Analysis Date = 06/25/15 Pct Recovery = 86% Analysis Date = 06/21/15 Pct Recovery = 86% Analysis Date = 06/21/15 Pct Recovery = 86% Analysis Date = 06/16/15 Pct Recovery = 86% Analysis Date = 06/16/15 Pct Recovery = 86% Analysis Date = 06/11/15 Pct Recovery = 86% Analysis Date = 06/11/15 Pct Recovery = 86% Analysis Date = 06/06/15 Pct Recovery = 86% Analysis Date = 06/06/15 Pct Recovery = 86% Analysis Date = 06/01/15 Pct Recovery = 86% Analysis Date = 06/01/15 Pct Recovery = 86% Analysis Date = 05/27/15 Pct Recovery = 86% Analysis Date = 05/27/15 Pct Recovery = 86% Analysis Date = 05/23/15 Pct Recovery = 86% Analysis Date = 05/23/15 Pct Recovery = 86% Analysis Date = 05/18/15 Pct Recovery = 86% Analysis Date = 05/18/15 Pct Recovery = 86% Analysis Date = 05/13/15 Pct Recovery = 86% Analysis Date = 05/13/15 Pct Recovery = 86% Analysis Date = 05/08/15 Pct Recovery = 86% Analysis Date = 05/08/15 Pct Recovery = 86% Analysis Date = 05/03/15 Pct Recovery = 86% Analysis Date = 05/03/15 Pct Recovery = 86% Analysis Date = 04/29/15 Pct Recovery = 86% Analysis Date = 04/29/15 Pct Recovery = 86% Analysis Date = 04/24/15 Pct Recovery = 86% Analysis Date = 04/24/15 Pct Recovery = 86% Analysis Date = 04/19/15 Pct Recovery = 86% Analysis Date = 04/19/15 Pct Recovery = 86% Analysis Date = 04/14/15 Pct Recovery = 86% Analysis Date = 04/14/15 Pct Recovery = 86% Analysis Date = 04/09/15 Pct Recovery = 86% Analysis Date = 04/09/15 Pct Recovery = 86% Analysis Date = 04/04/15 Pct Recovery = 86% Analysis Date = 04/04/15 Pct Recovery = 86% Analysis Date = 03/31/15 Pct Recovery = 86% Analysis Date = 03/31/15 Pct Recovery = 86% Analysis Date = 03/26/15 Pct Recovery = 86% Analysis Date = 03/26/15 Pct Recovery = 86% Analysis Date = 03/21/15 Pct Recovery = 86% Analysis Date = 03/21/15 Pct Recovery = 86% Analysis Date = 03/16/15 Pct Recovery = 86% Analysis Date = 03/16/15 Pct Recovery = 86% Analysis Date = 03/11/15 Pct Recovery = 86% Analysis Date = 03/11/15 Pct Recovery = 86% Analysis Date = 03/07/15 Pct Recovery = 86% Analysis Date = 03/07/15 Pct Recovery = 86% Analysis Date = 03/02/15 Pct Recovery = 86% Analysis Date = 03/02/15 Pct Recovery = 86% Analysis Date = 02/25/15 Pct Recovery = 86% Analysis Date = 02/25/15 Pct Recovery = 86% Analysis Date = 02/20/15 Pct Recovery = 86% Analysis Date = 02/20/15 Pct Recovery = 86% Analysis Date = 02/15/15 Pct Recovery = 86% Analysis Date = 02/15/15 Pct Recovery = 86% Analysis Date = 02/10/15 Pct Recovery = 86% Analysis Date = 02/10/15 Pct Recovery = 86% Analysis Date = 02/06/15 Pct Recovery = 86% Analysis Date = 02/06/15 Pct Recovery = 86% Analysis Date = 02/01/15 Pct Recovery = 86% Analysis Date = 02/01/15 Pct Recovery = 86% Analysis Date = 01/27/15 Pct Recovery = 86% Analysis Date = 01/27/15 Pct Recovery = 86% Analysis Date = 01/22/15 Pct Recovery = 86% Analysis Date = 01/22/15 Pct Recovery = 86% Analysis Date = 01/17/15 Pct Recovery = 86% Analysis Date = 01/17/15 Pct Recovery = 86% Analysis Date = 01/12/15 Pct Recovery = 86% Analysis Date = 01/12/15 Pct Recovery = 86% Analysis Date = 01/08/15 Pct Recovery = 86% Analysis Date = 01/08/15 Pct Recovery = 86% Analysis Date = 01/03/15 Pct Recovery = 86% Analysis Date = 01/03/15 Pct Recovery = 86% Analysis Date = 12/29/14 Pct Recovery = 86% Analysis Date = 12/29/14 Pct Recovery = 86% Analysis Date = 12/24/14 Pct Recovery = 86% Analysis Date = 12/24/14 Pct Recovery = 86% Analysis Date = 12/19/14 Pct Recovery = 86% Analysis Date = 12/19/14 Pct Recovery = 86% Analysis Date = 12/15/14 Pct Recovery = 86% Analysis Date = 12/15/14 Pct Recovery = 86% Analysis Date = 12/10/14 Pct Recovery = 86% Analysis Date = 12/10/14 Pct Recovery = 86% Analysis Date = 12/05/14 Pct Recovery = 86% Analysis Date = 12/05/14 Pct Recovery = 86% Analysis Date = 11/30/14 Pct Recovery = 86% Analysis Date = 11/30/14 Pct Recovery = 86% Analysis Date = 11/25/14 Pct Recovery = 86% Analysis Date = 11/25/14 Pct Recovery = 86% Analysis Date = 11/20/14 Pct Recovery = 86% Analysis Date = 11/20/14 Pct Recovery = 86% Analysis Date = 11/16/14 Pct Recovery = 86% Analysis Date = 11/16/14 Pct Recovery = 86% Analysis Date = 11/11/14 Pct Recovery = 86% Analysis Date = 11/11/14 Pct Recovery = 86% Analysis Date = 11/06/14 Pct Recovery = 86% Analysis Date = 11/06/14 Pct Recovery = 86% Analysis Date = 11/01/14 Pct Recovery = 86% Analysis Date = 11/01/14 Pct Recovery = 86% Analysis Date = 10/27/14 Pct Recovery = 86% Analysis Date = 10/27/14 Pct Recovery = 86% Analysis Date = 10/23/14 Pct Recovery = 86% Analysis Date = 10/23/14 Pct Recovery = 86% Analysis Date = 10/18/14 Pct Recovery = 86% Analysis Date = 10/18/14 Pct Recovery = 86% Analysis Date = 10/13/14 Pct Recovery = 86% Analysis Date = 10/13/14 Pct Recovery = 86% Analysis Date = 10/08/14 Pct Recovery = 86% Analysis Date = 10/08/14 Pct Recovery = 86% Analysis Date = 10/03/14 Pct Recovery = 86% Analysis Date = 10/03/14 Pct Recovery = 86% Analysis Date = 09/28/14 Pct Recovery = 86% Analysis Date = 09/28/14 Pct Recovery = 86% Analysis Date = 09/24/14 Pct Recovery = 86% Analysis Date = 09/24/14 Pct Recovery = 86% Analysis Date = 09/19/14 Pct Recovery = 86% Analysis Date = 09/19/14 Pct Recovery = 86% Analysis Date = 09/14/14 Pct Recovery = 86% Analysis Date = 09/14/14 Pct Recovery = 86% Analysis Date = 09/09/14 Pct Recovery = 86% Analysis Date = 09/09/14 Pct Recovery = 86% Analysis Date = 09/04/14 Pct Recovery = 86% Analysis Date = 09/04/14 Pct Recovery = 86% Analysis Date = 08/31/14 Pct Recovery = 86% Analysis Date = 08/31/14 Pct Recovery = 86% Analysis Date = 08/26/14 Pct Recovery = 86% Analysis Date = 08/26/14 Pct Recovery = 86% Analysis Date = 08/21/14 Pct Recovery = 86% Analysis Date = 08/21/14 Pct Recovery = 86% Analysis Date = 08/16/14 Pct Recovery = 86% Analysis Date = 08/16/14 Pct Recovery = 86% Analysis Date = 08/11/14 Pct Recovery = 86% Analysis Date = 08/11/14 Pct Recovery = 86% Analysis Date = 08/06/14 Pct Recovery = 86% Analysis Date = 08/06/14 Pct Recovery = 86% Analysis Date = 08/02/14 Pct Recovery = 86% Analysis Date = 08/02/14 Pct Recovery = 86% Analysis Date = 07/28/14 Pct Recovery = 86% Analysis Date = 07/28/14 Pct Recovery = 86% Analysis Date = 07/23/14 Pct Recovery = 86% Analysis Date = 07/23/14 Pct Recovery = 86% Analysis Date = 07/18/14 Pct Recovery = 86% Analysis Date = 07/18/14 Pct Recovery = 86% Analysis Date = 07/13/14 Pct Recovery = 86% Analysis Date = 07/13/14 Pct Recovery = 86% Analysis Date = 07/09/14 Pct Recovery = 86% Analysis Date = 07/09/14 Pct Recovery = 86% Analysis Date = 07/04/14 Pct Recovery = 86% Analysis Date = 07/04/14 Pct Recovery = 86% Analysis Date = 06/29/14 Pct Recovery = 86% Analysis Date = 06/29/14 Pct Recovery = 86% Analysis Date = 06/24/14 Pct Recovery = 86% Analysis Date = 06/24/14 Pct Recovery = 86% Analysis Date = 06/19/14 Pct Recovery = 86% Analysis Date = 06/19/14 Pct Recovery = 86% Analysis Date = 06/14/14 Pct Recovery = 86% Analysis Date = 06/14/14 Pct Recovery = 86% Analysis Date = 06/10/14 Pct Recovery = 86% Analysis Date = 06/10/14 Pct Recovery = 86% Analysis Date = 06/05/14 Pct Recovery = 86% Analysis Date = 06/05/14 Pct Recovery = 86% Analysis Date = 05/31/14 Pct Recovery = 86% Analysis Date = 05/31/14 Pct Recovery = 86% Analysis Date = 05/26/14 Pct Recovery = 86% Analysis Date = 05/26/14 Pct Recovery = 86% Analysis Date = 05/21/14 Pct Recovery = 86% Analysis Date = 05/21/14 Pct Recovery = 86% Analysis Date = 05/17/14 Pct Recovery = 86% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
HYDROCORTISONE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 67 83% 12% 82% 10%
Total 67 83% 12% 82% 10%

Sample Statistics
HYDROCORTISONE

Characteristic N % % Basis
Plotted 67 89% Spiked
Estimated Values 26 35% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 2 3% Spiked
Spiked 75 .  
False Negatives 6 8% 6 out of 75
Not Spiked 40 .  
False Positives 0 0% 0 out of 40

BQS OBSP Determination:
HYDROXYZINE
METHOD: 2440 , TESTIDCODE: 68005LCM56
Open Data Set

Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 437% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 431% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 366% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 366% Analysis Date = 09/24/16 SpikeMix = Crescent EN160610015: 80 µl & Abs 061416: 80 µl Pct Recovery = 433% Analysis Date = 09/24/16 SpikeMix = Abs 061416: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 467% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 428% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 396% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 453% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 502% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 64% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 73% Analysis Date = 01/17/16 SpikeMix = ERA 0406-15-09: 80 µl & ERA 0406-15-07A: 80 µl Pct Recovery = 66% Analysis Date = 11/24/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 77% Analysis Date = 10/01/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 113% Analysis Date = 11/05/15 SpikeMix = ERA 0406-15-08: 80 µl & Abs 052215: 80 µl Pct Recovery = 71% Analysis Date = 11/04/15 SpikeMix = Abs 052215: 80 µl & Abs 050115: 80 µl Pct Recovery = 69% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 64% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 62% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 75% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 76% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-04: 15 µl & Abs 041814: 15 µl Pct Recovery = 61% Analysis Date = 12/06/14 SpikeMix = ERA 0318-14-02: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 65% Analysis Date = 10/25/14 SpikeMix = Abs 041614: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 69% Analysis Date = 10/11/14 SpikeMix = ERA 0318-14-02: 60 µl & ERA 0319-14-04: 60 µl Pct Recovery = 60% Analysis Date = 08/28/14 SpikeMix = ERA 0319-14-04: 60 µl & ERA 0319-14-05: 60 µl Pct Recovery = 68% Analysis Date = 05/07/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 99% Analysis Date = 03/11/15 SpikeMix = ERA 0318-14-02: 15 µl & Abs 041714: 15 µl Pct Recovery = 90% Analysis Date = 01/16/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 77% Analysis Date = 12/06/14 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 67% Analysis Date = 08/21/14 SpikeMix = ERA 0318-14-02: 60 µl & Abs 041714: 60 µl Pct Recovery = 65% Analysis Date = 07/12/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 64% Analysis Date = 06/11/14 SpikeMix = Abs 041614: 60 µl & Abs 041714: 60 µl Pct Recovery = 64% Analysis Date = 05/21/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 77% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-08: 40 µl & ERA 0406-15-09: 40 µl Pct Recovery = 53% Analysis Date = 07/31/15 SpikeMix = ERA 0406-15-09: 40 µl & Abs 050115: 40 µl Pct Recovery = 61% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-08: 40 µl & Abs 052215: 40 µl Pct Recovery = 78% Analysis Date = 02/23/16 SpikeMix = Abs 052215: 40 µl & Abs 050115: 40 µl Pct Recovery = 74% Analysis Date = 09/10/15 SpikeMix = Abs 052215: 40 µl & ERA 0406-15-07A: 40 µl Pct Recovery = 70% Analysis Date = 07/31/15 SpikeMix = Abs 051315: 40 µl & Abs 052215: 40 µl Pct Recovery = 71% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 71% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 67% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 70% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 70% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 52% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 53% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 61% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 52% Analysis Date = 04/10/15 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 65% Analysis Date = 02/10/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 66% Analysis Date = 12/07/14 SpikeMix = ERA 0318-14-02: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 86% Analysis Date = 10/11/14 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 41% Analysis Date = 11/04/14 SpikeMix = Abs 041714: 8 µl & ERA 0319-14-05: 8 µl Pct Recovery = 43% Analysis Date = 04/23/14 SpikeMix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.2: 20 µl Pct Recovery = 67% Analysis Date = 09/12/14 SpikeMix = Abs 041614: 30 µl & ERA 0319-14-04: 30 µl Pct Recovery = 54% Analysis Date = 08/16/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 58% Analysis Date = 07/13/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 53% Analysis Date = 07/20/14 SpikeMix = ERA 0318-14-02: 30 µl & Abs 041714: 30 µl Pct Recovery = 65% Analysis Date = 06/28/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 59% Analysis Date = 05/17/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 72% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 51% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 70% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-08: 20 µl & ERA 0406-15-09: 20 µl Pct Recovery = 48% Analysis Date = 11/24/15 SpikeMix = ERA 0406-15-09: 20 µl & Abs 050115: 20 µl Pct Recovery = 72% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-09: 20 µl Pct Recovery = 85% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 55% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 59% Analysis Date = 02/23/16 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 84% Analysis Date = 11/24/15 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 78% Analysis Date = 09/09/15 SpikeMix = ERA 0406-15-08: 20 µl & Abs 052215: 20 µl Pct Recovery = 70% Analysis Date = 08/27/15 SpikeMix = Abs 052215: 20 µl & Abs 050115: 20 µl Pct Recovery = 79% Analysis Date = 07/09/15 SpikeMix = Abs 050115: 20 µl & Abs 052215: 20 µl Pct Recovery = 72% Analysis Date = 06/26/15 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 59% Analysis Date = 04/09/16 SpikeMix = Abs 051315: 10 µl & ERA 0406-15-09: 10 µl Pct Recovery = 7% Analysis Date = 09/15/16 Pct Recovery = 203% Analysis Date = 09/15/16 Pct Recovery = 203% Analysis Date = 09/10/16 Pct Recovery = 199% Analysis Date = 09/10/16 Pct Recovery = 199% Analysis Date = 09/05/16 Pct Recovery = 195% Analysis Date = 09/05/16 Pct Recovery = 195% Analysis Date = 08/31/16 Pct Recovery = 191% Analysis Date = 08/31/16 Pct Recovery = 191% Analysis Date = 08/26/16 Pct Recovery = 187% Analysis Date = 08/26/16 Pct Recovery = 187% Analysis Date = 08/21/16 Pct Recovery = 184% Analysis Date = 08/21/16 Pct Recovery = 184% Analysis Date = 08/16/16 Pct Recovery = 180% Analysis Date = 08/16/16 Pct Recovery = 180% Analysis Date = 08/11/16 Pct Recovery = 176% Analysis Date = 08/11/16 Pct Recovery = 176% Analysis Date = 08/06/16 Pct Recovery = 172% Analysis Date = 08/06/16 Pct Recovery = 172% Analysis Date = 08/01/16 Pct Recovery = 168% Analysis Date = 08/01/16 Pct Recovery = 168% Analysis Date = 07/27/16 Pct Recovery = 164% Analysis Date = 07/27/16 Pct Recovery = 164% Analysis Date = 07/22/16 Pct Recovery = 161% Analysis Date = 07/22/16 Pct Recovery = 161% Analysis Date = 07/17/16 Pct Recovery = 157% Analysis Date = 07/17/16 Pct Recovery = 157% Analysis Date = 07/12/16 Pct Recovery = 154% Analysis Date = 07/12/16 Pct Recovery = 154% Analysis Date = 07/07/16 Pct Recovery = 150% Analysis Date = 07/07/16 Pct Recovery = 150% Analysis Date = 07/02/16 Pct Recovery = 147% Analysis Date = 07/02/16 Pct Recovery = 147% Analysis Date = 06/27/16 Pct Recovery = 143% Analysis Date = 06/27/16 Pct Recovery = 143% Analysis Date = 06/22/16 Pct Recovery = 140% Analysis Date = 06/22/16 Pct Recovery = 140% Analysis Date = 06/17/16 Pct Recovery = 137% Analysis Date = 06/17/16 Pct Recovery = 137% Analysis Date = 06/12/16 Pct Recovery = 133% Analysis Date = 06/12/16 Pct Recovery = 133% Analysis Date = 06/07/16 Pct Recovery = 130% Analysis Date = 06/07/16 Pct Recovery = 130% Analysis Date = 06/02/16 Pct Recovery = 126% Analysis Date = 06/02/16 Pct Recovery = 126% Analysis Date = 05/28/16 Pct Recovery = 123% Analysis Date = 05/28/16 Pct Recovery = 123% Analysis Date = 05/23/16 Pct Recovery = 119% Analysis Date = 05/23/16 Pct Recovery = 119% Analysis Date = 05/18/16 Pct Recovery = 116% Analysis Date = 05/18/16 Pct Recovery = 116% Analysis Date = 05/13/16 Pct Recovery = 113% Analysis Date = 05/13/16 Pct Recovery = 113% Analysis Date = 05/08/16 Pct Recovery = 109% Analysis Date = 05/08/16 Pct Recovery = 109% Analysis Date = 05/03/16 Pct Recovery = 106% Analysis Date = 05/03/16 Pct Recovery = 106% Analysis Date = 04/28/16 Pct Recovery = 102% Analysis Date = 04/28/16 Pct Recovery = 102% Analysis Date = 04/23/16 Pct Recovery = 99% Analysis Date = 04/23/16 Pct Recovery = 99% Analysis Date = 04/18/16 Pct Recovery = 95% Analysis Date = 04/18/16 Pct Recovery = 95% Analysis Date = 04/13/16 Pct Recovery = 92% Analysis Date = 04/13/16 Pct Recovery = 92% Analysis Date = 04/08/16 Pct Recovery = 89% Analysis Date = 04/08/16 Pct Recovery = 89% Analysis Date = 04/03/16 Pct Recovery = 88% Analysis Date = 04/03/16 Pct Recovery = 88% Analysis Date = 03/29/16 Pct Recovery = 87% Analysis Date = 03/29/16 Pct Recovery = 87% Analysis Date = 03/24/16 Pct Recovery = 86% Analysis Date = 03/24/16 Pct Recovery = 86% Analysis Date = 03/19/16 Pct Recovery = 84% Analysis Date = 03/19/16 Pct Recovery = 84% Analysis Date = 03/14/16 Pct Recovery = 83% Analysis Date = 03/14/16 Pct Recovery = 83% Analysis Date = 03/09/16 Pct Recovery = 82% Analysis Date = 03/09/16 Pct Recovery = 82% Analysis Date = 03/04/16 Pct Recovery = 81% Analysis Date = 03/04/16 Pct Recovery = 81% Analysis Date = 02/28/16 Pct Recovery = 80% Analysis Date = 02/28/16 Pct Recovery = 80% Analysis Date = 02/23/16 Pct Recovery = 79% Analysis Date = 02/23/16 Pct Recovery = 79% Analysis Date = 02/18/16 Pct Recovery = 78% Analysis Date = 02/18/16 Pct Recovery = 78% Analysis Date = 02/13/16 Pct Recovery = 77% Analysis Date = 02/13/16 Pct Recovery = 77% Analysis Date = 02/08/16 Pct Recovery = 76% Analysis Date = 02/08/16 Pct Recovery = 76% Analysis Date = 02/03/16 Pct Recovery = 75% Analysis Date = 02/03/16 Pct Recovery = 75% Analysis Date = 01/29/16 Pct Recovery = 74% Analysis Date = 01/29/16 Pct Recovery = 74% Analysis Date = 01/24/16 Pct Recovery = 72% Analysis Date = 01/24/16 Pct Recovery = 72% Analysis Date = 01/19/16 Pct Recovery = 71% Analysis Date = 01/19/16 Pct Recovery = 71% Analysis Date = 01/14/16 Pct Recovery = 71% Analysis Date = 01/14/16 Pct Recovery = 71% Analysis Date = 01/09/16 Pct Recovery = 71% Analysis Date = 01/09/16 Pct Recovery = 71% Analysis Date = 01/04/16 Pct Recovery = 71% Analysis Date = 01/04/16 Pct Recovery = 71% Analysis Date = 12/30/15 Pct Recovery = 71% Analysis Date = 12/30/15 Pct Recovery = 71% Analysis Date = 12/25/15 Pct Recovery = 71% Analysis Date = 12/25/15 Pct Recovery = 71% Analysis Date = 12/20/15 Pct Recovery = 71% Analysis Date = 12/20/15 Pct Recovery = 71% Analysis Date = 12/15/15 Pct Recovery = 70% Analysis Date = 12/15/15 Pct Recovery = 70% Analysis Date = 12/10/15 Pct Recovery = 70% Analysis Date = 12/10/15 Pct Recovery = 70% Analysis Date = 12/05/15 Pct Recovery = 70% Analysis Date = 12/05/15 Pct Recovery = 70% Analysis Date = 11/30/15 Pct Recovery = 70% Analysis Date = 11/30/15 Pct Recovery = 70% Analysis Date = 11/25/15 Pct Recovery = 70% Analysis Date = 11/25/15 Pct Recovery = 70% Analysis Date = 11/20/15 Pct Recovery = 70% Analysis Date = 11/20/15 Pct Recovery = 70% Analysis Date = 11/15/15 Pct Recovery = 70% Analysis Date = 11/15/15 Pct Recovery = 70% Analysis Date = 11/10/15 Pct Recovery = 70% Analysis Date = 11/10/15 Pct Recovery = 70% Analysis Date = 11/05/15 Pct Recovery = 70% Analysis Date = 11/05/15 Pct Recovery = 70% Analysis Date = 10/31/15 Pct Recovery = 70% Analysis Date = 10/31/15 Pct Recovery = 70% Analysis Date = 10/26/15 Pct Recovery = 70% Analysis Date = 10/26/15 Pct Recovery = 70% Analysis Date = 10/21/15 Pct Recovery = 70% Analysis Date = 10/21/15 Pct Recovery = 70% Analysis Date = 10/16/15 Pct Recovery = 71% Analysis Date = 10/16/15 Pct Recovery = 71% Analysis Date = 10/11/15 Pct Recovery = 71% Analysis Date = 10/11/15 Pct Recovery = 71% Analysis Date = 10/06/15 Pct Recovery = 71% Analysis Date = 10/06/15 Pct Recovery = 71% Analysis Date = 10/01/15 Pct Recovery = 71% Analysis Date = 10/01/15 Pct Recovery = 71% Analysis Date = 09/26/15 Pct Recovery = 71% Analysis Date = 09/26/15 Pct Recovery = 71% Analysis Date = 09/21/15 Pct Recovery = 71% Analysis Date = 09/21/15 Pct Recovery = 71% Analysis Date = 09/16/15 Pct Recovery = 71% Analysis Date = 09/16/15 Pct Recovery = 71% Analysis Date = 09/11/15 Pct Recovery = 71% Analysis Date = 09/11/15 Pct Recovery = 71% Analysis Date = 09/05/15 Pct Recovery = 71% Analysis Date = 09/05/15 Pct Recovery = 71% Analysis Date = 08/31/15 Pct Recovery = 72% Analysis Date = 08/31/15 Pct Recovery = 72% Analysis Date = 08/26/15 Pct Recovery = 72% Analysis Date = 08/26/15 Pct Recovery = 72% Analysis Date = 08/21/15 Pct Recovery = 72% Analysis Date = 08/21/15 Pct Recovery = 72% Analysis Date = 08/16/15 Pct Recovery = 72% Analysis Date = 08/16/15 Pct Recovery = 72% Analysis Date = 08/11/15 Pct Recovery = 72% Analysis Date = 08/11/15 Pct Recovery = 72% Analysis Date = 08/06/15 Pct Recovery = 72% Analysis Date = 08/06/15 Pct Recovery = 72% Analysis Date = 08/01/15 Pct Recovery = 72% Analysis Date = 08/01/15 Pct Recovery = 72% Analysis Date = 07/27/15 Pct Recovery = 72% Analysis Date = 07/27/15 Pct Recovery = 72% Analysis Date = 07/22/15 Pct Recovery = 72% Analysis Date = 07/22/15 Pct Recovery = 72% Analysis Date = 07/17/15 Pct Recovery = 72% Analysis Date = 07/17/15 Pct Recovery = 72% Analysis Date = 07/12/15 Pct Recovery = 72% Analysis Date = 07/12/15 Pct Recovery = 72% Analysis Date = 07/07/15 Pct Recovery = 72% Analysis Date = 07/07/15 Pct Recovery = 72% Analysis Date = 07/02/15 Pct Recovery = 71% Analysis Date = 07/02/15 Pct Recovery = 71% Analysis Date = 06/27/15 Pct Recovery = 71% Analysis Date = 06/27/15 Pct Recovery = 71% Analysis Date = 06/22/15 Pct Recovery = 71% Analysis Date = 06/22/15 Pct Recovery = 71% Analysis Date = 06/17/15 Pct Recovery = 71% Analysis Date = 06/17/15 Pct Recovery = 71% Analysis Date = 06/12/15 Pct Recovery = 71% Analysis Date = 06/12/15 Pct Recovery = 71% Analysis Date = 06/07/15 Pct Recovery = 71% Analysis Date = 06/07/15 Pct Recovery = 71% Analysis Date = 06/02/15 Pct Recovery = 71% Analysis Date = 06/02/15 Pct Recovery = 71% Analysis Date = 05/28/15 Pct Recovery = 71% Analysis Date = 05/28/15 Pct Recovery = 71% Analysis Date = 05/23/15 Pct Recovery = 71% Analysis Date = 05/23/15 Pct Recovery = 71% Analysis Date = 05/18/15 Pct Recovery = 71% Analysis Date = 05/18/15 Pct Recovery = 71% Analysis Date = 05/13/15 Pct Recovery = 71% Analysis Date = 05/13/15 Pct Recovery = 71% Analysis Date = 05/08/15 Pct Recovery = 71% Analysis Date = 05/08/15 Pct Recovery = 71% Analysis Date = 05/03/15 Pct Recovery = 70% Analysis Date = 05/03/15 Pct Recovery = 70% Analysis Date = 04/28/15 Pct Recovery = 70% Analysis Date = 04/28/15 Pct Recovery = 70% Analysis Date = 04/23/15 Pct Recovery = 70% Analysis Date = 04/23/15 Pct Recovery = 70% Analysis Date = 04/18/15 Pct Recovery = 70% Analysis Date = 04/18/15 Pct Recovery = 70% Analysis Date = 04/13/15 Pct Recovery = 70% Analysis Date = 04/13/15 Pct Recovery = 70% Analysis Date = 04/08/15 Pct Recovery = 70% Analysis Date = 04/08/15 Pct Recovery = 70% Analysis Date = 04/03/15 Pct Recovery = 70% Analysis Date = 04/03/15 Pct Recovery = 70% Analysis Date = 03/29/15 Pct Recovery = 70% Analysis Date = 03/29/15 Pct Recovery = 70% Analysis Date = 03/24/15 Pct Recovery = 70% Analysis Date = 03/24/15 Pct Recovery = 70% Analysis Date = 03/19/15 Pct Recovery = 69% Analysis Date = 03/19/15 Pct Recovery = 69% Analysis Date = 03/14/15 Pct Recovery = 69% Analysis Date = 03/14/15 Pct Recovery = 69% Analysis Date = 03/09/15 Pct Recovery = 69% Analysis Date = 03/09/15 Pct Recovery = 69% Analysis Date = 03/04/15 Pct Recovery = 69% Analysis Date = 03/04/15 Pct Recovery = 69% Analysis Date = 02/27/15 Pct Recovery = 69% Analysis Date = 02/27/15 Pct Recovery = 69% Analysis Date = 02/22/15 Pct Recovery = 69% Analysis Date = 02/22/15 Pct Recovery = 69% Analysis Date = 02/17/15 Pct Recovery = 69% Analysis Date = 02/17/15 Pct Recovery = 69% Analysis Date = 02/12/15 Pct Recovery = 69% Analysis Date = 02/12/15 Pct Recovery = 69% Analysis Date = 02/07/15 Pct Recovery = 68% Analysis Date = 02/07/15 Pct Recovery = 68% Analysis Date = 02/02/15 Pct Recovery = 68% Analysis Date = 02/02/15 Pct Recovery = 68% Analysis Date = 01/28/15 Pct Recovery = 68% Analysis Date = 01/28/15 Pct Recovery = 68% Analysis Date = 01/23/15 Pct Recovery = 68% Analysis Date = 01/23/15 Pct Recovery = 68% Analysis Date = 01/18/15 Pct Recovery = 68% Analysis Date = 01/18/15 Pct Recovery = 68% Analysis Date = 01/13/15 Pct Recovery = 68% Analysis Date = 01/13/15 Pct Recovery = 68% Analysis Date = 01/08/15 Pct Recovery = 68% Analysis Date = 01/08/15 Pct Recovery = 68% Analysis Date = 01/03/15 Pct Recovery = 67% Analysis Date = 01/03/15 Pct Recovery = 67% Analysis Date = 12/29/14 Pct Recovery = 67% Analysis Date = 12/29/14 Pct Recovery = 67% Analysis Date = 12/24/14 Pct Recovery = 67% Analysis Date = 12/24/14 Pct Recovery = 67% Analysis Date = 12/19/14 Pct Recovery = 67% Analysis Date = 12/19/14 Pct Recovery = 67% Analysis Date = 12/14/14 Pct Recovery = 67% Analysis Date = 12/14/14 Pct Recovery = 67% Analysis Date = 12/09/14 Pct Recovery = 67% Analysis Date = 12/09/14 Pct Recovery = 67% Analysis Date = 12/04/14 Pct Recovery = 67% Analysis Date = 12/04/14 Pct Recovery = 67% Analysis Date = 11/29/14 Pct Recovery = 67% Analysis Date = 11/29/14 Pct Recovery = 67% Analysis Date = 11/24/14 Pct Recovery = 66% Analysis Date = 11/24/14 Pct Recovery = 66% Analysis Date = 11/19/14 Pct Recovery = 66% Analysis Date = 11/19/14 Pct Recovery = 66% Analysis Date = 11/14/14 Pct Recovery = 66% Analysis Date = 11/14/14 Pct Recovery = 66% Analysis Date = 11/09/14 Pct Recovery = 66% Analysis Date = 11/09/14 Pct Recovery = 66% Analysis Date = 11/04/14 Pct Recovery = 66% Analysis Date = 11/04/14 Pct Recovery = 66% Analysis Date = 10/30/14 Pct Recovery = 66% Analysis Date = 10/30/14 Pct Recovery = 66% Analysis Date = 10/25/14 Pct Recovery = 66% Analysis Date = 10/25/14 Pct Recovery = 66% Analysis Date = 10/20/14 Pct Recovery = 66% Analysis Date = 10/20/14 Pct Recovery = 66% Analysis Date = 10/15/14 Pct Recovery = 66% Analysis Date = 10/15/14 Pct Recovery = 66% Analysis Date = 10/10/14 Pct Recovery = 65% Analysis Date = 10/10/14 Pct Recovery = 65% Analysis Date = 10/05/14 Pct Recovery = 65% Analysis Date = 10/05/14 Pct Recovery = 65% Analysis Date = 09/30/14 Pct Recovery = 65% Analysis Date = 09/30/14 Pct Recovery = 65% Analysis Date = 09/25/14 Pct Recovery = 65% Analysis Date = 09/25/14 Pct Recovery = 65% Analysis Date = 09/20/14 Pct Recovery = 65% Analysis Date = 09/20/14 Pct Recovery = 65% Analysis Date = 09/15/14 Pct Recovery = 65% Analysis Date = 09/15/14 Pct Recovery = 65% Analysis Date = 09/10/14 Pct Recovery = 65% Analysis Date = 09/10/14 Pct Recovery = 65% Analysis Date = 09/05/14 Pct Recovery = 65% Analysis Date = 09/05/14 Pct Recovery = 65% Analysis Date = 08/31/14 Pct Recovery = 64% Analysis Date = 08/31/14 Pct Recovery = 64% Analysis Date = 08/26/14 Pct Recovery = 64% Analysis Date = 08/26/14 Pct Recovery = 64% Analysis Date = 08/21/14 Pct Recovery = 64% Analysis Date = 08/21/14 Pct Recovery = 64% Analysis Date = 08/16/14 Pct Recovery = 64% Analysis Date = 08/16/14 Pct Recovery = 64% Analysis Date = 08/11/14 Pct Recovery = 64% Analysis Date = 08/11/14 Pct Recovery = 64% Analysis Date = 08/06/14 Pct Recovery = 64% Analysis Date = 08/06/14 Pct Recovery = 64% Analysis Date = 08/01/14 Pct Recovery = 64% Analysis Date = 08/01/14 Pct Recovery = 64% Analysis Date = 07/27/14 Pct Recovery = 64% Analysis Date = 07/27/14 Pct Recovery = 64% Analysis Date = 07/22/14 Pct Recovery = 63% Analysis Date = 07/22/14 Pct Recovery = 63% Analysis Date = 07/17/14 Pct Recovery = 63% Analysis Date = 07/17/14 Pct Recovery = 63% Analysis Date = 07/12/14 Pct Recovery = 63% Analysis Date = 07/12/14 Pct Recovery = 63% Analysis Date = 07/07/14 Pct Recovery = 63% Analysis Date = 07/07/14 Pct Recovery = 63% Analysis Date = 07/02/14 Pct Recovery = 63% Analysis Date = 07/02/14 Pct Recovery = 63% Analysis Date = 06/27/14 Pct Recovery = 63% Analysis Date = 06/27/14 Pct Recovery = 63% Analysis Date = 06/22/14 Pct Recovery = 63% Analysis Date = 06/22/14 Pct Recovery = 63% Analysis Date = 06/17/14 Pct Recovery = 63% Analysis Date = 06/17/14 Pct Recovery = 63% Analysis Date = 06/12/14 Pct Recovery = 62% Analysis Date = 06/12/14 Pct Recovery = 62% Analysis Date = 06/07/14 Pct Recovery = 62% Analysis Date = 06/07/14 Pct Recovery = 62% Analysis Date = 06/02/14 Pct Recovery = 62% Analysis Date = 06/02/14 Pct Recovery = 62% Analysis Date = 05/28/14 Pct Recovery = 62% Analysis Date = 05/28/14 Pct Recovery = 62% Analysis Date = 05/23/14 Pct Recovery = 62% Analysis Date = 05/23/14 Pct Recovery = 62% Analysis Date = 05/18/14 Pct Recovery = 62% Analysis Date = 05/18/14 Pct Recovery = 62% Analysis Date = 05/13/14 Pct Recovery = 62% Analysis Date = 05/13/14 Pct Recovery = 62% Analysis Date = 05/08/14 Pct Recovery = 62% Analysis Date = 05/08/14 Pct Recovery = 62% Analysis Date = 05/03/14 Pct Recovery = 61% Analysis Date = 05/03/14 Pct Recovery = 61% Analysis Date = 04/28/14 Pct Recovery = 61% Analysis Date = 04/28/14 Pct Recovery = 61% Analysis Date = 04/23/14 Pct Recovery = 61% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
HYDROXYZINE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 1 7% . 7% 0%
>= Reporting Level 73 117% 126% 70% 12%
Total 74 115% 126% 70% 13%

Sample Statistics
HYDROXYZINE

Characteristic N % % Basis
Plotted 74 96% Spiked
Estimated Values 6 8% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 1 1% Spiked
Spiked 77 .  
False Negatives 2 3% 2 out of 77
Not Spiked 38 .  
False Positives 0 0% 0 out of 38

BQS OBSP Determination:
IMINOSTILBENE
METHOD: 2440 , TESTIDCODE: 67481LCM56
Open Data Set

Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 102% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 102% Analysis Date = 01/17/16 SpikeMix = ERA 0406-15-09: 80 µl & ERA 0406-15-07A: 80 µl Pct Recovery = 72% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 80 µl & Abs 051315: 80 µl Pct Recovery = 65% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 80 µl & ERA 0406-15-08: 80 µl Pct Recovery = 75% Analysis Date = 11/04/15 SpikeMix = Abs 052215: 80 µl & Abs 050115: 80 µl Pct Recovery = 39% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 79% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 82% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 47% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 72% Analysis Date = 11/18/16 SpikeMix = ERA 04281604: 80 µl & ERA 04281603: 80 µl Pct Recovery = 72% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & ERA 04281604: 80 µl Pct Recovery = 72% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 67% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 68% Analysis Date = 05/07/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 117% Analysis Date = 04/29/15 SpikeMix = ERA 0319-14-05: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 119% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 115% Analysis Date = 01/16/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 99% Analysis Date = 12/07/14 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 74% Analysis Date = 12/06/14 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 84% Analysis Date = 08/28/14 SpikeMix = ERA 0319-14-04: 60 µl & ERA 0319-14-05: 60 µl Pct Recovery = 79% Analysis Date = 07/26/14 SpikeMix = ERA 0319-14-05: 60 µl & ERA 0318-14-02: 60 µl Pct Recovery = 104% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-04: 15 µl & Abs 041814: 15 µl Pct Recovery = 113% Analysis Date = 02/06/15 SpikeMix = Abs 041814: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 108% Analysis Date = 07/12/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 116% Analysis Date = 06/22/14 SpikeMix = Abs 041814: 60 µl & Abs 041614: 60 µl Pct Recovery = 109% Analysis Date = 05/21/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 101% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-07A: 40 µl & Abs 051315: 40 µl Pct Recovery = 67% Analysis Date = 11/04/15 SpikeMix = ERA 0406-15-07A: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 80% Analysis Date = 09/10/15 SpikeMix = Abs 052215: 40 µl & ERA 0406-15-07A: 40 µl Pct Recovery = 85% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 64% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 56% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 27% Analysis Date = 02/23/16 SpikeMix = Abs 052215: 40 µl & Abs 050115: 40 µl Pct Recovery = 35% Analysis Date = 07/31/15 SpikeMix = ERA 0406-15-09: 40 µl & Abs 050115: 40 µl Pct Recovery = 41% Analysis Date = 07/30/15 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 45% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 121% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 122% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 92% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 87% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 93% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 93% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 58% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 64% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 59% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 62% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 72% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 80% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 61% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 63% Analysis Date = 11/04/14 SpikeMix = Abs 041714: 8 µl & ERA 0319-14-05: 8 µl Pct Recovery = 27% Analysis Date = 10/24/14 SpikeMix = ERA 0319-14-05: 8 µl & Abs 041614: 8 µl Pct Recovery = 65% Analysis Date = 04/10/15 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 98% Analysis Date = 11/04/14 SpikeMix = Abs 041814: 8 µl & ERA 0318-14-02: 8 µl Pct Recovery = 63% Analysis Date = 10/11/14 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 52% Analysis Date = 08/30/14 SpikeMix = ERA 0318-14-02: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 91% Analysis Date = 08/16/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 65% Analysis Date = 07/13/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 123% Analysis Date = 10/10/14 SpikeMix = Abs 041714: 30 µl & Abs 041814: 30 µl Pct Recovery = 92% Analysis Date = 10/10/14 SpikeMix = Abs 041814: 30 µl & ERA 0318-14-02: 30 µl Pct Recovery = 98% Analysis Date = 07/13/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 124% Analysis Date = 05/30/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 101% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 66% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 59% Analysis Date = 04/27/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 106% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 97% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 93% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 72% Analysis Date = 11/24/15 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 80% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-09: 20 µl Pct Recovery = 65% Analysis Date = 09/15/15 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 79% Analysis Date = 11/25/15 SpikeMix = Abs 050115: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 29% Analysis Date = 11/24/15 SpikeMix = ERA 0406-15-09: 20 µl & Abs 050115: 20 µl Pct Recovery = 36% Analysis Date = 08/27/15 SpikeMix = Abs 052215: 20 µl & Abs 050115: 20 µl Pct Recovery = 44% Analysis Date = 08/11/15 SpikeMix = Abs 050115: 20 µl & Abs 051315: 20 µl Pct Recovery = 30% Analysis Date = 07/09/15 SpikeMix = Abs 050115: 20 µl & Abs 052215: 20 µl Pct Recovery = 43% Analysis Date = 06/09/15 SpikeMix = Abs 051315: 20 µl & Abs 050115: 20 µl Pct Recovery = 46% Analysis Date = 01/18/17 Pct Recovery = 92% Analysis Date = 01/14/17 Pct Recovery = 91% Analysis Date = 01/14/17 Pct Recovery = 91% Analysis Date = 01/09/17 Pct Recovery = 91% Analysis Date = 01/09/17 Pct Recovery = 91% Analysis Date = 01/04/17 Pct Recovery = 90% Analysis Date = 01/04/17 Pct Recovery = 90% Analysis Date = 12/30/16 Pct Recovery = 89% Analysis Date = 12/30/16 Pct Recovery = 89% Analysis Date = 12/25/16 Pct Recovery = 89% Analysis Date = 12/25/16 Pct Recovery = 89% Analysis Date = 12/20/16 Pct Recovery = 88% Analysis Date = 12/20/16 Pct Recovery = 88% Analysis Date = 12/15/16 Pct Recovery = 88% Analysis Date = 12/15/16 Pct Recovery = 88% Analysis Date = 12/11/16 Pct Recovery = 87% Analysis Date = 12/11/16 Pct Recovery = 87% Analysis Date = 12/06/16 Pct Recovery = 87% Analysis Date = 12/06/16 Pct Recovery = 87% Analysis Date = 12/01/16 Pct Recovery = 86% Analysis Date = 12/01/16 Pct Recovery = 86% Analysis Date = 11/26/16 Pct Recovery = 86% Analysis Date = 11/26/16 Pct Recovery = 86% Analysis Date = 11/21/16 Pct Recovery = 85% Analysis Date = 11/21/16 Pct Recovery = 85% Analysis Date = 11/16/16 Pct Recovery = 85% Analysis Date = 11/16/16 Pct Recovery = 85% Analysis Date = 11/11/16 Pct Recovery = 84% Analysis Date = 11/11/16 Pct Recovery = 84% Analysis Date = 11/06/16 Pct Recovery = 84% Analysis Date = 11/06/16 Pct Recovery = 84% Analysis Date = 11/02/16 Pct Recovery = 83% Analysis Date = 11/02/16 Pct Recovery = 83% Analysis Date = 10/28/16 Pct Recovery = 83% Analysis Date = 10/28/16 Pct Recovery = 83% Analysis Date = 10/23/16 Pct Recovery = 82% Analysis Date = 10/23/16 Pct Recovery = 82% Analysis Date = 10/18/16 Pct Recovery = 82% Analysis Date = 10/18/16 Pct Recovery = 82% Analysis Date = 10/13/16 Pct Recovery = 81% Analysis Date = 10/13/16 Pct Recovery = 81% Analysis Date = 10/08/16 Pct Recovery = 81% Analysis Date = 10/08/16 Pct Recovery = 81% Analysis Date = 10/03/16 Pct Recovery = 80% Analysis Date = 10/03/16 Pct Recovery = 80% Analysis Date = 09/28/16 Pct Recovery = 80% Analysis Date = 09/28/16 Pct Recovery = 80% Analysis Date = 09/24/16 Pct Recovery = 79% Analysis Date = 09/24/16 Pct Recovery = 79% Analysis Date = 09/19/16 Pct Recovery = 79% Analysis Date = 09/19/16 Pct Recovery = 79% Analysis Date = 09/14/16 Pct Recovery = 78% Analysis Date = 09/14/16 Pct Recovery = 78% Analysis Date = 09/09/16 Pct Recovery = 78% Analysis Date = 09/09/16 Pct Recovery = 78% Analysis Date = 09/04/16 Pct Recovery = 77% Analysis Date = 09/04/16 Pct Recovery = 77% Analysis Date = 08/30/16 Pct Recovery = 77% Analysis Date = 08/30/16 Pct Recovery = 77% Analysis Date = 08/25/16 Pct Recovery = 76% Analysis Date = 08/25/16 Pct Recovery = 76% Analysis Date = 08/21/16 Pct Recovery = 76% Analysis Date = 08/21/16 Pct Recovery = 76% Analysis Date = 08/16/16 Pct Recovery = 75% Analysis Date = 08/16/16 Pct Recovery = 75% Analysis Date = 08/11/16 Pct Recovery = 75% Analysis Date = 08/11/16 Pct Recovery = 75% Analysis Date = 08/06/16 Pct Recovery = 75% Analysis Date = 08/06/16 Pct Recovery = 75% Analysis Date = 08/01/16 Pct Recovery = 74% Analysis Date = 08/01/16 Pct Recovery = 74% Analysis Date = 07/27/16 Pct Recovery = 74% Analysis Date = 07/27/16 Pct Recovery = 74% Analysis Date = 07/22/16 Pct Recovery = 73% Analysis Date = 07/22/16 Pct Recovery = 73% Analysis Date = 07/17/16 Pct Recovery = 73% Analysis Date = 07/17/16 Pct Recovery = 73% Analysis Date = 07/13/16 Pct Recovery = 73% Analysis Date = 07/13/16 Pct Recovery = 73% Analysis Date = 07/08/16 Pct Recovery = 72% Analysis Date = 07/08/16 Pct Recovery = 72% Analysis Date = 07/03/16 Pct Recovery = 72% Analysis Date = 07/03/16 Pct Recovery = 72% Analysis Date = 06/28/16 Pct Recovery = 72% Analysis Date = 06/28/16 Pct Recovery = 72% Analysis Date = 06/23/16 Pct Recovery = 71% Analysis Date = 06/23/16 Pct Recovery = 71% Analysis Date = 06/18/16 Pct Recovery = 71% Analysis Date = 06/18/16 Pct Recovery = 71% Analysis Date = 06/13/16 Pct Recovery = 70% Analysis Date = 06/13/16 Pct Recovery = 70% Analysis Date = 06/08/16 Pct Recovery = 70% Analysis Date = 06/08/16 Pct Recovery = 70% Analysis Date = 06/04/16 Pct Recovery = 70% Analysis Date = 06/04/16 Pct Recovery = 70% Analysis Date = 05/30/16 Pct Recovery = 69% Analysis Date = 05/30/16 Pct Recovery = 69% Analysis Date = 05/25/16 Pct Recovery = 69% Analysis Date = 05/25/16 Pct Recovery = 69% Analysis Date = 05/20/16 Pct Recovery = 68% Analysis Date = 05/20/16 Pct Recovery = 68% Analysis Date = 05/15/16 Pct Recovery = 68% Analysis Date = 05/15/16 Pct Recovery = 68% Analysis Date = 05/10/16 Pct Recovery = 68% Analysis Date = 05/10/16 Pct Recovery = 68% Analysis Date = 05/05/16 Pct Recovery = 67% Analysis Date = 05/05/16 Pct Recovery = 67% Analysis Date = 05/01/16 Pct Recovery = 67% Analysis Date = 05/01/16 Pct Recovery = 67% Analysis Date = 04/26/16 Pct Recovery = 67% Analysis Date = 04/26/16 Pct Recovery = 67% Analysis Date = 04/21/16 Pct Recovery = 66% Analysis Date = 04/21/16 Pct Recovery = 66% Analysis Date = 04/16/16 Pct Recovery = 66% Analysis Date = 04/16/16 Pct Recovery = 66% Analysis Date = 04/11/16 Pct Recovery = 66% Analysis Date = 04/11/16 Pct Recovery = 66% Analysis Date = 04/06/16 Pct Recovery = 66% Analysis Date = 04/06/16 Pct Recovery = 66% Analysis Date = 04/01/16 Pct Recovery = 66% Analysis Date = 04/01/16 Pct Recovery = 66% Analysis Date = 03/27/16 Pct Recovery = 65% Analysis Date = 03/27/16 Pct Recovery = 65% Analysis Date = 03/23/16 Pct Recovery = 65% Analysis Date = 03/23/16 Pct Recovery = 65% Analysis Date = 03/18/16 Pct Recovery = 65% Analysis Date = 03/18/16 Pct Recovery = 65% Analysis Date = 03/13/16 Pct Recovery = 65% Analysis Date = 03/13/16 Pct Recovery = 65% Analysis Date = 03/08/16 Pct Recovery = 65% Analysis Date = 03/08/16 Pct Recovery = 65% Analysis Date = 03/03/16 Pct Recovery = 65% Analysis Date = 03/03/16 Pct Recovery = 65% Analysis Date = 02/27/16 Pct Recovery = 64% Analysis Date = 02/27/16 Pct Recovery = 64% Analysis Date = 02/22/16 Pct Recovery = 64% Analysis Date = 02/22/16 Pct Recovery = 64% Analysis Date = 02/17/16 Pct Recovery = 64% Analysis Date = 02/17/16 Pct Recovery = 64% Analysis Date = 02/13/16 Pct Recovery = 64% Analysis Date = 02/13/16 Pct Recovery = 64% Analysis Date = 02/08/16 Pct Recovery = 64% Analysis Date = 02/08/16 Pct Recovery = 64% Analysis Date = 02/03/16 Pct Recovery = 64% Analysis Date = 02/03/16 Pct Recovery = 64% Analysis Date = 01/29/16 Pct Recovery = 64% Analysis Date = 01/29/16 Pct Recovery = 64% Analysis Date = 01/24/16 Pct Recovery = 63% Analysis Date = 01/24/16 Pct Recovery = 63% Analysis Date = 01/19/16 Pct Recovery = 63% Analysis Date = 01/19/16 Pct Recovery = 63% Analysis Date = 01/14/16 Pct Recovery = 63% Analysis Date = 01/14/16 Pct Recovery = 63% Analysis Date = 01/10/16 Pct Recovery = 63% Analysis Date = 01/10/16 Pct Recovery = 63% Analysis Date = 01/05/16 Pct Recovery = 63% Analysis Date = 01/05/16 Pct Recovery = 63% Analysis Date = 12/31/15 Pct Recovery = 63% Analysis Date = 12/31/15 Pct Recovery = 63% Analysis Date = 12/26/15 Pct Recovery = 63% Analysis Date = 12/26/15 Pct Recovery = 63% Analysis Date = 12/21/15 Pct Recovery = 63% Analysis Date = 12/21/15 Pct Recovery = 63% Analysis Date = 12/16/15 Pct Recovery = 63% Analysis Date = 12/16/15 Pct Recovery = 63% Analysis Date = 12/11/15 Pct Recovery = 62% Analysis Date = 12/11/15 Pct Recovery = 62% Analysis Date = 12/06/15 Pct Recovery = 62% Analysis Date = 12/06/15 Pct Recovery = 62% Analysis Date = 12/02/15 Pct Recovery = 62% Analysis Date = 12/02/15 Pct Recovery = 62% Analysis Date = 11/27/15 Pct Recovery = 62% Analysis Date = 11/27/15 Pct Recovery = 62% Analysis Date = 11/22/15 Pct Recovery = 62% Analysis Date = 11/22/15 Pct Recovery = 62% Analysis Date = 11/17/15 Pct Recovery = 62% Analysis Date = 11/17/15 Pct Recovery = 62% Analysis Date = 11/12/15 Pct Recovery = 63% Analysis Date = 11/12/15 Pct Recovery = 63% Analysis Date = 11/07/15 Pct Recovery = 63% Analysis Date = 11/07/15 Pct Recovery = 63% Analysis Date = 11/02/15 Pct Recovery = 64% Analysis Date = 11/02/15 Pct Recovery = 64% Analysis Date = 10/28/15 Pct Recovery = 64% Analysis Date = 10/28/15 Pct Recovery = 64% Analysis Date = 10/24/15 Pct Recovery = 64% Analysis Date = 10/24/15 Pct Recovery = 64% Analysis Date = 10/19/15 Pct Recovery = 65% Analysis Date = 10/19/15 Pct Recovery = 65% Analysis Date = 10/14/15 Pct Recovery = 65% Analysis Date = 10/14/15 Pct Recovery = 65% Analysis Date = 10/09/15 Pct Recovery = 66% Analysis Date = 10/09/15 Pct Recovery = 66% Analysis Date = 10/04/15 Pct Recovery = 66% Analysis Date = 10/04/15 Pct Recovery = 66% Analysis Date = 09/29/15 Pct Recovery = 66% Analysis Date = 09/29/15 Pct Recovery = 66% Analysis Date = 09/24/15 Pct Recovery = 67% Analysis Date = 09/24/15 Pct Recovery = 67% Analysis Date = 09/19/15 Pct Recovery = 67% Analysis Date = 09/19/15 Pct Recovery = 67% Analysis Date = 09/15/15 Pct Recovery = 67% Analysis Date = 09/15/15 Pct Recovery = 67% Analysis Date = 09/10/15 Pct Recovery = 68% Analysis Date = 09/10/15 Pct Recovery = 68% Analysis Date = 09/05/15 Pct Recovery = 68% Analysis Date = 09/05/15 Pct Recovery = 68% Analysis Date = 08/31/15 Pct Recovery = 69% Analysis Date = 08/31/15 Pct Recovery = 69% Analysis Date = 08/26/15 Pct Recovery = 69% Analysis Date = 08/26/15 Pct Recovery = 69% Analysis Date = 08/21/15 Pct Recovery = 69% Analysis Date = 08/21/15 Pct Recovery = 69% Analysis Date = 08/16/15 Pct Recovery = 70% Analysis Date = 08/16/15 Pct Recovery = 70% Analysis Date = 08/12/15 Pct Recovery = 70% Analysis Date = 08/12/15 Pct Recovery = 70% Analysis Date = 08/07/15 Pct Recovery = 70% Analysis Date = 08/07/15 Pct Recovery = 70% Analysis Date = 08/02/15 Pct Recovery = 71% Analysis Date = 08/02/15 Pct Recovery = 71% Analysis Date = 07/28/15 Pct Recovery = 71% Analysis Date = 07/28/15 Pct Recovery = 71% Analysis Date = 07/23/15 Pct Recovery = 71% Analysis Date = 07/23/15 Pct Recovery = 71% Analysis Date = 07/18/15 Pct Recovery = 71% Analysis Date = 07/18/15 Pct Recovery = 71% Analysis Date = 07/13/15 Pct Recovery = 71% Analysis Date = 07/13/15 Pct Recovery = 71% Analysis Date = 07/08/15 Pct Recovery = 72% Analysis Date = 07/08/15 Pct Recovery = 72% Analysis Date = 07/04/15 Pct Recovery = 72% Analysis Date = 07/04/15 Pct Recovery = 72% Analysis Date = 06/29/15 Pct Recovery = 72% Analysis Date = 06/29/15 Pct Recovery = 72% Analysis Date = 06/24/15 Pct Recovery = 72% Analysis Date = 06/24/15 Pct Recovery = 72% Analysis Date = 06/19/15 Pct Recovery = 72% Analysis Date = 06/19/15 Pct Recovery = 72% Analysis Date = 06/14/15 Pct Recovery = 73% Analysis Date = 06/14/15 Pct Recovery = 73% Analysis Date = 06/09/15 Pct Recovery = 73% Analysis Date = 06/09/15 Pct Recovery = 73% Analysis Date = 06/04/15 Pct Recovery = 73% Analysis Date = 06/04/15 Pct Recovery = 73% Analysis Date = 05/30/15 Pct Recovery = 73% Analysis Date = 05/30/15 Pct Recovery = 73% Analysis Date = 05/26/15 Pct Recovery = 73% Analysis Date = 05/26/15 Pct Recovery = 73% Analysis Date = 05/21/15 Pct Recovery = 74% Analysis Date = 05/21/15 Pct Recovery = 74% Analysis Date = 05/16/15 Pct Recovery = 74% Analysis Date = 05/16/15 Pct Recovery = 74% Analysis Date = 05/11/15 Pct Recovery = 74% Analysis Date = 05/11/15 Pct Recovery = 74% Analysis Date = 05/06/15 Pct Recovery = 74% Analysis Date = 05/06/15 Pct Recovery = 74% Analysis Date = 05/01/15 Pct Recovery = 75% Analysis Date = 05/01/15 Pct Recovery = 75% Analysis Date = 04/26/15 Pct Recovery = 75% Analysis Date = 04/26/15 Pct Recovery = 75% Analysis Date = 04/22/15 Pct Recovery = 75% Analysis Date = 04/22/15 Pct Recovery = 75% Analysis Date = 04/17/15 Pct Recovery = 76% Analysis Date = 04/17/15 Pct Recovery = 76% Analysis Date = 04/12/15 Pct Recovery = 76% Analysis Date = 04/12/15 Pct Recovery = 76% Analysis Date = 04/07/15 Pct Recovery = 76% Analysis Date = 04/07/15 Pct Recovery = 76% Analysis Date = 04/02/15 Pct Recovery = 77% Analysis Date = 04/02/15 Pct Recovery = 77% Analysis Date = 03/28/15 Pct Recovery = 77% Analysis Date = 03/28/15 Pct Recovery = 77% Analysis Date = 03/23/15 Pct Recovery = 77% Analysis Date = 03/23/15 Pct Recovery = 77% Analysis Date = 03/18/15 Pct Recovery = 78% Analysis Date = 03/18/15 Pct Recovery = 78% Analysis Date = 03/14/15 Pct Recovery = 78% Analysis Date = 03/14/15 Pct Recovery = 78% Analysis Date = 03/09/15 Pct Recovery = 78% Analysis Date = 03/09/15 Pct Recovery = 78% Analysis Date = 03/04/15 Pct Recovery = 79% Analysis Date = 03/04/15 Pct Recovery = 79% Analysis Date = 02/27/15 Pct Recovery = 79% Analysis Date = 02/27/15 Pct Recovery = 79% Analysis Date = 02/22/15 Pct Recovery = 79% Analysis Date = 02/22/15 Pct Recovery = 79% Analysis Date = 02/17/15 Pct Recovery = 80% Analysis Date = 02/17/15 Pct Recovery = 80% Analysis Date = 02/12/15 Pct Recovery = 80% Analysis Date = 02/12/15 Pct Recovery = 80% Analysis Date = 02/07/15 Pct Recovery = 81% Analysis Date = 02/07/15 Pct Recovery = 81% Analysis Date = 02/03/15 Pct Recovery = 81% Analysis Date = 02/03/15 Pct Recovery = 81% Analysis Date = 01/29/15 Pct Recovery = 81% Analysis Date = 01/29/15 Pct Recovery = 81% Analysis Date = 01/24/15 Pct Recovery = 82% Analysis Date = 01/24/15 Pct Recovery = 82% Analysis Date = 01/19/15 Pct Recovery = 82% Analysis Date = 01/19/15 Pct Recovery = 82% Analysis Date = 01/14/15 Pct Recovery = 83% Analysis Date = 01/14/15 Pct Recovery = 83% Analysis Date = 01/09/15 Pct Recovery = 83% Analysis Date = 01/09/15 Pct Recovery = 83% Analysis Date = 01/04/15 Pct Recovery = 83% Analysis Date = 01/04/15 Pct Recovery = 83% Analysis Date = 12/31/14 Pct Recovery = 84% Analysis Date = 12/31/14 Pct Recovery = 84% Analysis Date = 12/26/14 Pct Recovery = 84% Analysis Date = 12/26/14 Pct Recovery = 84% Analysis Date = 12/21/14 Pct Recovery = 85% Analysis Date = 12/21/14 Pct Recovery = 85% Analysis Date = 12/16/14 Pct Recovery = 85% Analysis Date = 12/16/14 Pct Recovery = 85% Analysis Date = 12/11/14 Pct Recovery = 85% Analysis Date = 12/11/14 Pct Recovery = 85% Analysis Date = 12/06/14 Pct Recovery = 86% Analysis Date = 12/06/14 Pct Recovery = 86% Analysis Date = 12/01/14 Pct Recovery = 86% Analysis Date = 12/01/14 Pct Recovery = 86% Analysis Date = 11/26/14 Pct Recovery = 87% Analysis Date = 11/26/14 Pct Recovery = 87% Analysis Date = 11/22/14 Pct Recovery = 87% Analysis Date = 11/22/14 Pct Recovery = 87% Analysis Date = 11/17/14 Pct Recovery = 87% Analysis Date = 11/17/14 Pct Recovery = 87% Analysis Date = 11/12/14 Pct Recovery = 88% Analysis Date = 11/12/14 Pct Recovery = 88% Analysis Date = 11/07/14 Pct Recovery = 88% Analysis Date = 11/07/14 Pct Recovery = 88% Analysis Date = 11/02/14 Pct Recovery = 89% Analysis Date = 11/02/14 Pct Recovery = 89% Analysis Date = 10/28/14 Pct Recovery = 89% Analysis Date = 10/28/14 Pct Recovery = 89% Analysis Date = 10/23/14 Pct Recovery = 89% Analysis Date = 10/23/14 Pct Recovery = 89% Analysis Date = 10/18/14 Pct Recovery = 90% Analysis Date = 10/18/14 Pct Recovery = 90% Analysis Date = 10/14/14 Pct Recovery = 90% Analysis Date = 10/14/14 Pct Recovery = 90% Analysis Date = 10/09/14 Pct Recovery = 90% Analysis Date = 10/09/14 Pct Recovery = 90% Analysis Date = 10/04/14 Pct Recovery = 91% Analysis Date = 10/04/14 Pct Recovery = 91% Analysis Date = 09/29/14 Pct Recovery = 91% Analysis Date = 09/29/14 Pct Recovery = 91% Analysis Date = 09/24/14 Pct Recovery = 92% Analysis Date = 09/24/14 Pct Recovery = 92% Analysis Date = 09/19/14 Pct Recovery = 92% Analysis Date = 09/19/14 Pct Recovery = 92% Analysis Date = 09/14/14 Pct Recovery = 92% Analysis Date = 09/14/14 Pct Recovery = 92% Analysis Date = 09/10/14 Pct Recovery = 93% Analysis Date = 09/10/14 Pct Recovery = 93% Analysis Date = 09/05/14 Pct Recovery = 93% Analysis Date = 09/05/14 Pct Recovery = 93% Analysis Date = 08/31/14 Pct Recovery = 93% Analysis Date = 08/31/14 Pct Recovery = 93% Analysis Date = 08/26/14 Pct Recovery = 94% Analysis Date = 08/26/14 Pct Recovery = 94% Analysis Date = 08/21/14 Pct Recovery = 94% Analysis Date = 08/21/14 Pct Recovery = 94% Analysis Date = 08/16/14 Pct Recovery = 94% Analysis Date = 08/16/14 Pct Recovery = 94% Analysis Date = 08/11/14 Pct Recovery = 95% Analysis Date = 08/11/14 Pct Recovery = 95% Analysis Date = 08/06/14 Pct Recovery = 95% Analysis Date = 08/06/14 Pct Recovery = 95% Analysis Date = 08/02/14 Pct Recovery = 95% Analysis Date = 08/02/14 Pct Recovery = 95% Analysis Date = 07/28/14 Pct Recovery = 96% Analysis Date = 07/28/14 Pct Recovery = 96% Analysis Date = 07/23/14 Pct Recovery = 96% Analysis Date = 07/23/14 Pct Recovery = 96% Analysis Date = 07/18/14 Pct Recovery = 96% Analysis Date = 07/18/14 Pct Recovery = 96% Analysis Date = 07/13/14 Pct Recovery = 97% Analysis Date = 07/13/14 Pct Recovery = 97% Analysis Date = 07/08/14 Pct Recovery = 97% Analysis Date = 07/08/14 Pct Recovery = 97% Analysis Date = 07/03/14 Pct Recovery = 97% Analysis Date = 07/03/14 Pct Recovery = 97% Analysis Date = 06/28/14 Pct Recovery = 98% Analysis Date = 06/28/14 Pct Recovery = 98% Analysis Date = 06/24/14 Pct Recovery = 98% Analysis Date = 06/24/14 Pct Recovery = 98% Analysis Date = 06/19/14 Pct Recovery = 98% Analysis Date = 06/19/14 Pct Recovery = 98% Analysis Date = 06/14/14 Pct Recovery = 99% Analysis Date = 06/14/14 Pct Recovery = 99% Analysis Date = 06/09/14 Pct Recovery = 99% Analysis Date = 06/09/14 Pct Recovery = 99% Analysis Date = 06/04/14 Pct Recovery = 100% Analysis Date = 06/04/14 Pct Recovery = 100% Analysis Date = 05/30/14 Pct Recovery = 100% Analysis Date = 05/30/14 Pct Recovery = 100% Analysis Date = 05/25/14 Pct Recovery = 100% Analysis Date = 05/25/14 Pct Recovery = 100% Analysis Date = 05/21/14 Pct Recovery = 101% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
IMINOSTILBENE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 77 77% 26% 74% 27%
Total 77 77% 26% 74% 27%

Sample Statistics
IMINOSTILBENE

Characteristic N % % Basis
Plotted 77 100% Spiked
Estimated Values 11 14% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 77 .  
False Negatives 0 0% 0 out of 77
Not Spiked 38 .  
False Positives 0 0% 0 out of 38

BQS OBSP Determination:
KETOCONAZOLE
METHOD: 2440 , TESTIDCODE: 68014LCM56
Open Data Set

Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 48% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 53% Analysis Date = 11/05/15 SpikeMix = ERA 0406-15-08: 80 µl & Abs 052215: 80 µl Pct Recovery = 41% Analysis Date = 11/04/15 SpikeMix = Abs 052215: 80 µl & Abs 050115: 80 µl Pct Recovery = 42% Analysis Date = 01/17/16 SpikeMix = ERA 0406-15-09: 80 µl & ERA 0406-15-07A: 80 µl Pct Recovery = 46% Analysis Date = 11/24/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 47% Analysis Date = 10/01/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 71% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 59% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 58% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 36% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 52% Analysis Date = 11/18/16 SpikeMix = ERA 04281604: 80 µl & ERA 04281603: 80 µl Pct Recovery = 58% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & ERA 04281604: 80 µl Pct Recovery = 53% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 53% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 53% Analysis Date = 05/07/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 39% Analysis Date = 04/29/15 SpikeMix = ERA 0319-14-05: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 60% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 41% Analysis Date = 01/16/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 31% Analysis Date = 12/07/14 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 34% Analysis Date = 12/06/14 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 45% Analysis Date = 08/28/14 SpikeMix = ERA 0319-14-04: 60 µl & ERA 0319-14-05: 60 µl Pct Recovery = 53% Analysis Date = 07/26/14 SpikeMix = ERA 0319-14-05: 60 µl & ERA 0318-14-02: 60 µl Pct Recovery = 73% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-04: 15 µl & Abs 041814: 15 µl Pct Recovery = 38% Analysis Date = 02/06/15 SpikeMix = Abs 041814: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 29% Analysis Date = 07/12/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 50% Analysis Date = 06/22/14 SpikeMix = Abs 041814: 60 µl & Abs 041614: 60 µl Pct Recovery = 81% Analysis Date = 05/21/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 82% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-08: 40 µl & Abs 052215: 40 µl Pct Recovery = 44% Analysis Date = 02/23/16 SpikeMix = Abs 052215: 40 µl & Abs 050115: 40 µl Pct Recovery = 59% Analysis Date = 09/10/15 SpikeMix = Abs 052215: 40 µl & ERA 0406-15-07A: 40 µl Pct Recovery = 57% Analysis Date = 07/31/15 SpikeMix = Abs 051315: 40 µl & Abs 052215: 40 µl Pct Recovery = 27% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-08: 40 µl & ERA 0406-15-09: 40 µl Pct Recovery = 40% Analysis Date = 07/31/15 SpikeMix = ERA 0406-15-09: 40 µl & Abs 050115: 40 µl Pct Recovery = 46% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 60% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 94% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 60% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 54% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 52% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 61% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 37% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 54% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 51% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 45% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 36% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 36% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 33% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 42% Analysis Date = 10/24/14 SpikeMix = ERA 0319-14-05: 8 µl & Abs 041614: 8 µl Pct Recovery = 12% Analysis Date = 04/10/15 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 23% Analysis Date = 10/11/14 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 12% Analysis Date = 08/30/14 SpikeMix = ERA 0318-14-02: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 59% Analysis Date = 08/16/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 31% Analysis Date = 07/13/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 35% Analysis Date = 10/10/14 SpikeMix = Abs 041714: 30 µl & Abs 041814: 30 µl Pct Recovery = 73% Analysis Date = 10/10/14 SpikeMix = Abs 041814: 30 µl & ERA 0318-14-02: 30 µl Pct Recovery = 66% Analysis Date = 07/13/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 48% Analysis Date = 05/30/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 59% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 22% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 26% Analysis Date = 02/23/16 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 35% Analysis Date = 11/24/15 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 23% Analysis Date = 09/09/15 SpikeMix = ERA 0406-15-08: 20 µl & Abs 052215: 20 µl Pct Recovery = 54% Analysis Date = 08/27/15 SpikeMix = Abs 052215: 20 µl & Abs 050115: 20 µl Pct Recovery = 21% Analysis Date = 07/09/15 SpikeMix = Abs 050115: 20 µl & Abs 052215: 20 µl Pct Recovery = 45% Analysis Date = 06/26/15 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 28% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 26% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 39% Analysis Date = 11/24/15 SpikeMix = ERA 0406-15-09: 20 µl & Abs 050115: 20 µl Pct Recovery = 42% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-09: 20 µl Pct Recovery = 45% Analysis Date = 04/09/16 SpikeMix = Abs 051315: 10 µl & ERA 0406-15-09: 10 µl Pct Recovery = 44% Analysis Date = 04/09/16 SpikeMix = Abs 051315: 10 µl & ERA 0406-15-09: 10 µl Pct Recovery = 34% Analysis Date = 01/18/17 Pct Recovery = 59% Analysis Date = 01/14/17 Pct Recovery = 58% Analysis Date = 01/14/17 Pct Recovery = 58% Analysis Date = 01/09/17 Pct Recovery = 58% Analysis Date = 01/09/17 Pct Recovery = 58% Analysis Date = 01/04/17 Pct Recovery = 58% Analysis Date = 01/04/17 Pct Recovery = 58% Analysis Date = 12/30/16 Pct Recovery = 57% Analysis Date = 12/30/16 Pct Recovery = 57% Analysis Date = 12/25/16 Pct Recovery = 57% Analysis Date = 12/25/16 Pct Recovery = 57% Analysis Date = 12/20/16 Pct Recovery = 56% Analysis Date = 12/20/16 Pct Recovery = 56% Analysis Date = 12/15/16 Pct Recovery = 56% Analysis Date = 12/15/16 Pct Recovery = 56% Analysis Date = 12/11/16 Pct Recovery = 56% Analysis Date = 12/11/16 Pct Recovery = 56% Analysis Date = 12/06/16 Pct Recovery = 55% Analysis Date = 12/06/16 Pct Recovery = 55% Analysis Date = 12/01/16 Pct Recovery = 55% Analysis Date = 12/01/16 Pct Recovery = 55% Analysis Date = 11/26/16 Pct Recovery = 55% Analysis Date = 11/26/16 Pct Recovery = 55% Analysis Date = 11/21/16 Pct Recovery = 54% Analysis Date = 11/21/16 Pct Recovery = 54% Analysis Date = 11/16/16 Pct Recovery = 54% Analysis Date = 11/16/16 Pct Recovery = 54% Analysis Date = 11/11/16 Pct Recovery = 53% Analysis Date = 11/11/16 Pct Recovery = 53% Analysis Date = 11/06/16 Pct Recovery = 53% Analysis Date = 11/06/16 Pct Recovery = 53% Analysis Date = 11/02/16 Pct Recovery = 53% Analysis Date = 11/02/16 Pct Recovery = 53% Analysis Date = 10/28/16 Pct Recovery = 52% Analysis Date = 10/28/16 Pct Recovery = 52% Analysis Date = 10/23/16 Pct Recovery = 52% Analysis Date = 10/23/16 Pct Recovery = 52% Analysis Date = 10/18/16 Pct Recovery = 52% Analysis Date = 10/18/16 Pct Recovery = 52% Analysis Date = 10/13/16 Pct Recovery = 51% Analysis Date = 10/13/16 Pct Recovery = 51% Analysis Date = 10/08/16 Pct Recovery = 51% Analysis Date = 10/08/16 Pct Recovery = 51% Analysis Date = 10/03/16 Pct Recovery = 51% Analysis Date = 10/03/16 Pct Recovery = 51% Analysis Date = 09/28/16 Pct Recovery = 50% Analysis Date = 09/28/16 Pct Recovery = 50% Analysis Date = 09/24/16 Pct Recovery = 50% Analysis Date = 09/24/16 Pct Recovery = 50% Analysis Date = 09/19/16 Pct Recovery = 50% Analysis Date = 09/19/16 Pct Recovery = 50% Analysis Date = 09/14/16 Pct Recovery = 49% Analysis Date = 09/14/16 Pct Recovery = 49% Analysis Date = 09/09/16 Pct Recovery = 49% Analysis Date = 09/09/16 Pct Recovery = 49% Analysis Date = 09/04/16 Pct Recovery = 49% Analysis Date = 09/04/16 Pct Recovery = 49% Analysis Date = 08/30/16 Pct Recovery = 48% Analysis Date = 08/30/16 Pct Recovery = 48% Analysis Date = 08/25/16 Pct Recovery = 48% Analysis Date = 08/25/16 Pct Recovery = 48% Analysis Date = 08/21/16 Pct Recovery = 48% Analysis Date = 08/21/16 Pct Recovery = 48% Analysis Date = 08/16/16 Pct Recovery = 47% Analysis Date = 08/16/16 Pct Recovery = 47% Analysis Date = 08/11/16 Pct Recovery = 47% Analysis Date = 08/11/16 Pct Recovery = 47% Analysis Date = 08/06/16 Pct Recovery = 47% Analysis Date = 08/06/16 Pct Recovery = 47% Analysis Date = 08/01/16 Pct Recovery = 46% Analysis Date = 08/01/16 Pct Recovery = 46% Analysis Date = 07/27/16 Pct Recovery = 46% Analysis Date = 07/27/16 Pct Recovery = 46% Analysis Date = 07/22/16 Pct Recovery = 46% Analysis Date = 07/22/16 Pct Recovery = 46% Analysis Date = 07/17/16 Pct Recovery = 45% Analysis Date = 07/17/16 Pct Recovery = 45% Analysis Date = 07/13/16 Pct Recovery = 45% Analysis Date = 07/13/16 Pct Recovery = 45% Analysis Date = 07/08/16 Pct Recovery = 45% Analysis Date = 07/08/16 Pct Recovery = 45% Analysis Date = 07/03/16 Pct Recovery = 45% Analysis Date = 07/03/16 Pct Recovery = 45% Analysis Date = 06/28/16 Pct Recovery = 45% Analysis Date = 06/28/16 Pct Recovery = 45% Analysis Date = 06/23/16 Pct Recovery = 44% Analysis Date = 06/23/16 Pct Recovery = 44% Analysis Date = 06/18/16 Pct Recovery = 44% Analysis Date = 06/18/16 Pct Recovery = 44% Analysis Date = 06/13/16 Pct Recovery = 44% Analysis Date = 06/13/16 Pct Recovery = 44% Analysis Date = 06/08/16 Pct Recovery = 44% Analysis Date = 06/08/16 Pct Recovery = 44% Analysis Date = 06/04/16 Pct Recovery = 44% Analysis Date = 06/04/16 Pct Recovery = 44% Analysis Date = 05/30/16 Pct Recovery = 43% Analysis Date = 05/30/16 Pct Recovery = 43% Analysis Date = 05/25/16 Pct Recovery = 43% Analysis Date = 05/25/16 Pct Recovery = 43% Analysis Date = 05/20/16 Pct Recovery = 43% Analysis Date = 05/20/16 Pct Recovery = 43% Analysis Date = 05/15/16 Pct Recovery = 43% Analysis Date = 05/15/16 Pct Recovery = 43% Analysis Date = 05/10/16 Pct Recovery = 43% Analysis Date = 05/10/16 Pct Recovery = 43% Analysis Date = 05/05/16 Pct Recovery = 43% Analysis Date = 05/05/16 Pct Recovery = 43% Analysis Date = 05/01/16 Pct Recovery = 42% Analysis Date = 05/01/16 Pct Recovery = 42% Analysis Date = 04/26/16 Pct Recovery = 42% Analysis Date = 04/26/16 Pct Recovery = 42% Analysis Date = 04/21/16 Pct Recovery = 42% Analysis Date = 04/21/16 Pct Recovery = 42% Analysis Date = 04/16/16 Pct Recovery = 42% Analysis Date = 04/16/16 Pct Recovery = 42% Analysis Date = 04/11/16 Pct Recovery = 42% Analysis Date = 04/11/16 Pct Recovery = 42% Analysis Date = 04/06/16 Pct Recovery = 41% Analysis Date = 04/06/16 Pct Recovery = 41% Analysis Date = 04/01/16 Pct Recovery = 41% Analysis Date = 04/01/16 Pct Recovery = 41% Analysis Date = 03/27/16 Pct Recovery = 41% Analysis Date = 03/27/16 Pct Recovery = 41% Analysis Date = 03/23/16 Pct Recovery = 41% Analysis Date = 03/23/16 Pct Recovery = 41% Analysis Date = 03/18/16 Pct Recovery = 41% Analysis Date = 03/18/16 Pct Recovery = 41% Analysis Date = 03/13/16 Pct Recovery = 41% Analysis Date = 03/13/16 Pct Recovery = 41% Analysis Date = 03/08/16 Pct Recovery = 41% Analysis Date = 03/08/16 Pct Recovery = 41% Analysis Date = 03/03/16 Pct Recovery = 41% Analysis Date = 03/03/16 Pct Recovery = 41% Analysis Date = 02/27/16 Pct Recovery = 41% Analysis Date = 02/27/16 Pct Recovery = 41% Analysis Date = 02/22/16 Pct Recovery = 41% Analysis Date = 02/22/16 Pct Recovery = 41% Analysis Date = 02/17/16 Pct Recovery = 41% Analysis Date = 02/17/16 Pct Recovery = 41% Analysis Date = 02/13/16 Pct Recovery = 41% Analysis Date = 02/13/16 Pct Recovery = 41% Analysis Date = 02/08/16 Pct Recovery = 41% Analysis Date = 02/08/16 Pct Recovery = 41% Analysis Date = 02/03/16 Pct Recovery = 41% Analysis Date = 02/03/16 Pct Recovery = 41% Analysis Date = 01/29/16 Pct Recovery = 41% Analysis Date = 01/29/16 Pct Recovery = 41% Analysis Date = 01/24/16 Pct Recovery = 41% Analysis Date = 01/24/16 Pct Recovery = 41% Analysis Date = 01/19/16 Pct Recovery = 41% Analysis Date = 01/19/16 Pct Recovery = 41% Analysis Date = 01/14/16 Pct Recovery = 41% Analysis Date = 01/14/16 Pct Recovery = 41% Analysis Date = 01/10/16 Pct Recovery = 41% Analysis Date = 01/10/16 Pct Recovery = 41% Analysis Date = 01/05/16 Pct Recovery = 41% Analysis Date = 01/05/16 Pct Recovery = 41% Analysis Date = 12/31/15 Pct Recovery = 41% Analysis Date = 12/31/15 Pct Recovery = 41% Analysis Date = 12/26/15 Pct Recovery = 41% Analysis Date = 12/26/15 Pct Recovery = 41% Analysis Date = 12/21/15 Pct Recovery = 41% Analysis Date = 12/21/15 Pct Recovery = 41% Analysis Date = 12/16/15 Pct Recovery = 41% Analysis Date = 12/16/15 Pct Recovery = 41% Analysis Date = 12/11/15 Pct Recovery = 41% Analysis Date = 12/11/15 Pct Recovery = 41% Analysis Date = 12/06/15 Pct Recovery = 41% Analysis Date = 12/06/15 Pct Recovery = 41% Analysis Date = 12/02/15 Pct Recovery = 41% Analysis Date = 12/02/15 Pct Recovery = 41% Analysis Date = 11/27/15 Pct Recovery = 41% Analysis Date = 11/27/15 Pct Recovery = 41% Analysis Date = 11/22/15 Pct Recovery = 41% Analysis Date = 11/22/15 Pct Recovery = 41% Analysis Date = 11/17/15 Pct Recovery = 41% Analysis Date = 11/17/15 Pct Recovery = 41% Analysis Date = 11/12/15 Pct Recovery = 41% Analysis Date = 11/12/15 Pct Recovery = 41% Analysis Date = 11/07/15 Pct Recovery = 41% Analysis Date = 11/07/15 Pct Recovery = 41% Analysis Date = 11/02/15 Pct Recovery = 41% Analysis Date = 11/02/15 Pct Recovery = 41% Analysis Date = 10/28/15 Pct Recovery = 41% Analysis Date = 10/28/15 Pct Recovery = 41% Analysis Date = 10/24/15 Pct Recovery = 41% Analysis Date = 10/24/15 Pct Recovery = 41% Analysis Date = 10/19/15 Pct Recovery = 41% Analysis Date = 10/19/15 Pct Recovery = 41% Analysis Date = 10/14/15 Pct Recovery = 41% Analysis Date = 10/14/15 Pct Recovery = 41% Analysis Date = 10/09/15 Pct Recovery = 41% Analysis Date = 10/09/15 Pct Recovery = 41% Analysis Date = 10/04/15 Pct Recovery = 41% Analysis Date = 10/04/15 Pct Recovery = 41% Analysis Date = 09/29/15 Pct Recovery = 41% Analysis Date = 09/29/15 Pct Recovery = 41% Analysis Date = 09/24/15 Pct Recovery = 41% Analysis Date = 09/24/15 Pct Recovery = 41% Analysis Date = 09/19/15 Pct Recovery = 41% Analysis Date = 09/19/15 Pct Recovery = 41% Analysis Date = 09/15/15 Pct Recovery = 41% Analysis Date = 09/15/15 Pct Recovery = 41% Analysis Date = 09/10/15 Pct Recovery = 41% Analysis Date = 09/10/15 Pct Recovery = 41% Analysis Date = 09/05/15 Pct Recovery = 41% Analysis Date = 09/05/15 Pct Recovery = 41% Analysis Date = 08/31/15 Pct Recovery = 41% Analysis Date = 08/31/15 Pct Recovery = 41% Analysis Date = 08/26/15 Pct Recovery = 41% Analysis Date = 08/26/15 Pct Recovery = 41% Analysis Date = 08/21/15 Pct Recovery = 41% Analysis Date = 08/21/15 Pct Recovery = 41% Analysis Date = 08/16/15 Pct Recovery = 41% Analysis Date = 08/16/15 Pct Recovery = 41% Analysis Date = 08/12/15 Pct Recovery = 41% Analysis Date = 08/12/15 Pct Recovery = 41% Analysis Date = 08/07/15 Pct Recovery = 41% Analysis Date = 08/07/15 Pct Recovery = 41% Analysis Date = 08/02/15 Pct Recovery = 41% Analysis Date = 08/02/15 Pct Recovery = 41% Analysis Date = 07/28/15 Pct Recovery = 41% Analysis Date = 07/28/15 Pct Recovery = 41% Analysis Date = 07/23/15 Pct Recovery = 41% Analysis Date = 07/23/15 Pct Recovery = 41% Analysis Date = 07/18/15 Pct Recovery = 41% Analysis Date = 07/18/15 Pct Recovery = 41% Analysis Date = 07/13/15 Pct Recovery = 41% Analysis Date = 07/13/15 Pct Recovery = 41% Analysis Date = 07/08/15 Pct Recovery = 41% Analysis Date = 07/08/15 Pct Recovery = 41% Analysis Date = 07/04/15 Pct Recovery = 40% Analysis Date = 07/04/15 Pct Recovery = 40% Analysis Date = 06/29/15 Pct Recovery = 40% Analysis Date = 06/29/15 Pct Recovery = 40% Analysis Date = 06/24/15 Pct Recovery = 40% Analysis Date = 06/24/15 Pct Recovery = 40% Analysis Date = 06/19/15 Pct Recovery = 40% Analysis Date = 06/19/15 Pct Recovery = 40% Analysis Date = 06/14/15 Pct Recovery = 40% Analysis Date = 06/14/15 Pct Recovery = 40% Analysis Date = 06/09/15 Pct Recovery = 40% Analysis Date = 06/09/15 Pct Recovery = 40% Analysis Date = 06/04/15 Pct Recovery = 40% Analysis Date = 06/04/15 Pct Recovery = 40% Analysis Date = 05/30/15 Pct Recovery = 40% Analysis Date = 05/30/15 Pct Recovery = 40% Analysis Date = 05/26/15 Pct Recovery = 40% Analysis Date = 05/26/15 Pct Recovery = 40% Analysis Date = 05/21/15 Pct Recovery = 40% Analysis Date = 05/21/15 Pct Recovery = 40% Analysis Date = 05/16/15 Pct Recovery = 40% Analysis Date = 05/16/15 Pct Recovery = 40% Analysis Date = 05/11/15 Pct Recovery = 40% Analysis Date = 05/11/15 Pct Recovery = 40% Analysis Date = 05/06/15 Pct Recovery = 40% Analysis Date = 05/06/15 Pct Recovery = 40% Analysis Date = 05/01/15 Pct Recovery = 41% Analysis Date = 05/01/15 Pct Recovery = 41% Analysis Date = 04/26/15 Pct Recovery = 41% Analysis Date = 04/26/15 Pct Recovery = 41% Analysis Date = 04/22/15 Pct Recovery = 41% Analysis Date = 04/22/15 Pct Recovery = 41% Analysis Date = 04/17/15 Pct Recovery = 41% Analysis Date = 04/17/15 Pct Recovery = 41% Analysis Date = 04/12/15 Pct Recovery = 41% Analysis Date = 04/12/15 Pct Recovery = 41% Analysis Date = 04/07/15 Pct Recovery = 41% Analysis Date = 04/07/15 Pct Recovery = 41% Analysis Date = 04/02/15 Pct Recovery = 41% Analysis Date = 04/02/15 Pct Recovery = 41% Analysis Date = 03/28/15 Pct Recovery = 42% Analysis Date = 03/28/15 Pct Recovery = 42% Analysis Date = 03/23/15 Pct Recovery = 42% Analysis Date = 03/23/15 Pct Recovery = 42% Analysis Date = 03/18/15 Pct Recovery = 42% Analysis Date = 03/18/15 Pct Recovery = 42% Analysis Date = 03/14/15 Pct Recovery = 42% Analysis Date = 03/14/15 Pct Recovery = 42% Analysis Date = 03/09/15 Pct Recovery = 42% Analysis Date = 03/09/15 Pct Recovery = 42% Analysis Date = 03/04/15 Pct Recovery = 42% Analysis Date = 03/04/15 Pct Recovery = 42% Analysis Date = 02/27/15 Pct Recovery = 43% Analysis Date = 02/27/15 Pct Recovery = 43% Analysis Date = 02/22/15 Pct Recovery = 43% Analysis Date = 02/22/15 Pct Recovery = 43% Analysis Date = 02/17/15 Pct Recovery = 43% Analysis Date = 02/17/15 Pct Recovery = 43% Analysis Date = 02/12/15 Pct Recovery = 43% Analysis Date = 02/12/15 Pct Recovery = 43% Analysis Date = 02/07/15 Pct Recovery = 43% Analysis Date = 02/07/15 Pct Recovery = 43% Analysis Date = 02/03/15 Pct Recovery = 43% Analysis Date = 02/03/15 Pct Recovery = 43% Analysis Date = 01/29/15 Pct Recovery = 44% Analysis Date = 01/29/15 Pct Recovery = 44% Analysis Date = 01/24/15 Pct Recovery = 44% Analysis Date = 01/24/15 Pct Recovery = 44% Analysis Date = 01/19/15 Pct Recovery = 44% Analysis Date = 01/19/15 Pct Recovery = 44% Analysis Date = 01/14/15 Pct Recovery = 44% Analysis Date = 01/14/15 Pct Recovery = 44% Analysis Date = 01/09/15 Pct Recovery = 45% Analysis Date = 01/09/15 Pct Recovery = 45% Analysis Date = 01/04/15 Pct Recovery = 45% Analysis Date = 01/04/15 Pct Recovery = 45% Analysis Date = 12/31/14 Pct Recovery = 45% Analysis Date = 12/31/14 Pct Recovery = 45% Analysis Date = 12/26/14 Pct Recovery = 45% Analysis Date = 12/26/14 Pct Recovery = 45% Analysis Date = 12/21/14 Pct Recovery = 45% Analysis Date = 12/21/14 Pct Recovery = 45% Analysis Date = 12/16/14 Pct Recovery = 46% Analysis Date = 12/16/14 Pct Recovery = 46% Analysis Date = 12/11/14 Pct Recovery = 46% Analysis Date = 12/11/14 Pct Recovery = 46% Analysis Date = 12/06/14 Pct Recovery = 46% Analysis Date = 12/06/14 Pct Recovery = 46% Analysis Date = 12/01/14 Pct Recovery = 46% Analysis Date = 12/01/14 Pct Recovery = 46% Analysis Date = 11/26/14 Pct Recovery = 46% Analysis Date = 11/26/14 Pct Recovery = 46% Analysis Date = 11/22/14 Pct Recovery = 47% Analysis Date = 11/22/14 Pct Recovery = 47% Analysis Date = 11/17/14 Pct Recovery = 47% Analysis Date = 11/17/14 Pct Recovery = 47% Analysis Date = 11/12/14 Pct Recovery = 47% Analysis Date = 11/12/14 Pct Recovery = 47% Analysis Date = 11/07/14 Pct Recovery = 47% Analysis Date = 11/07/14 Pct Recovery = 47% Analysis Date = 11/02/14 Pct Recovery = 48% Analysis Date = 11/02/14 Pct Recovery = 48% Analysis Date = 10/28/14 Pct Recovery = 48% Analysis Date = 10/28/14 Pct Recovery = 48% Analysis Date = 10/23/14 Pct Recovery = 48% Analysis Date = 10/23/14 Pct Recovery = 48% Analysis Date = 10/18/14 Pct Recovery = 48% Analysis Date = 10/18/14 Pct Recovery = 48% Analysis Date = 10/14/14 Pct Recovery = 48% Analysis Date = 10/14/14 Pct Recovery = 48% Analysis Date = 10/09/14 Pct Recovery = 49% Analysis Date = 10/09/14 Pct Recovery = 49% Analysis Date = 10/04/14 Pct Recovery = 49% Analysis Date = 10/04/14 Pct Recovery = 49% Analysis Date = 09/29/14 Pct Recovery = 49% Analysis Date = 09/29/14 Pct Recovery = 49% Analysis Date = 09/24/14 Pct Recovery = 49% Analysis Date = 09/24/14 Pct Recovery = 49% Analysis Date = 09/19/14 Pct Recovery = 50% Analysis Date = 09/19/14 Pct Recovery = 50% Analysis Date = 09/14/14 Pct Recovery = 50% Analysis Date = 09/14/14 Pct Recovery = 50% Analysis Date = 09/10/14 Pct Recovery = 50% Analysis Date = 09/10/14 Pct Recovery = 50% Analysis Date = 09/05/14 Pct Recovery = 50% Analysis Date = 09/05/14 Pct Recovery = 50% Analysis Date = 08/31/14 Pct Recovery = 51% Analysis Date = 08/31/14 Pct Recovery = 51% Analysis Date = 08/26/14 Pct Recovery = 51% Analysis Date = 08/26/14 Pct Recovery = 51% Analysis Date = 08/21/14 Pct Recovery = 51% Analysis Date = 08/21/14 Pct Recovery = 51% Analysis Date = 08/16/14 Pct Recovery = 51% Analysis Date = 08/16/14 Pct Recovery = 51% Analysis Date = 08/11/14 Pct Recovery = 51% Analysis Date = 08/11/14 Pct Recovery = 51% Analysis Date = 08/06/14 Pct Recovery = 52% Analysis Date = 08/06/14 Pct Recovery = 52% Analysis Date = 08/02/14 Pct Recovery = 52% Analysis Date = 08/02/14 Pct Recovery = 52% Analysis Date = 07/28/14 Pct Recovery = 52% Analysis Date = 07/28/14 Pct Recovery = 52% Analysis Date = 07/23/14 Pct Recovery = 52% Analysis Date = 07/23/14 Pct Recovery = 52% Analysis Date = 07/18/14 Pct Recovery = 53% Analysis Date = 07/18/14 Pct Recovery = 53% Analysis Date = 07/13/14 Pct Recovery = 53% Analysis Date = 07/13/14 Pct Recovery = 53% Analysis Date = 07/08/14 Pct Recovery = 53% Analysis Date = 07/08/14 Pct Recovery = 53% Analysis Date = 07/03/14 Pct Recovery = 54% Analysis Date = 07/03/14 Pct Recovery = 54% Analysis Date = 06/28/14 Pct Recovery = 54% Analysis Date = 06/28/14 Pct Recovery = 54% Analysis Date = 06/24/14 Pct Recovery = 54% Analysis Date = 06/24/14 Pct Recovery = 54% Analysis Date = 06/19/14 Pct Recovery = 54% Analysis Date = 06/19/14 Pct Recovery = 54% Analysis Date = 06/14/14 Pct Recovery = 55% Analysis Date = 06/14/14 Pct Recovery = 55% Analysis Date = 06/09/14 Pct Recovery = 55% Analysis Date = 06/09/14 Pct Recovery = 55% Analysis Date = 06/04/14 Pct Recovery = 55% Analysis Date = 06/04/14 Pct Recovery = 55% Analysis Date = 05/30/14 Pct Recovery = 55% Analysis Date = 05/30/14 Pct Recovery = 55% Analysis Date = 05/25/14 Pct Recovery = 56% Analysis Date = 05/25/14 Pct Recovery = 56% Analysis Date = 05/21/14 Pct Recovery = 56% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
KETOCONAZOLE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 2 39% 7% 39% 7%
>= Reporting Level 70 46% 16% 46% 16%
Total 72 46% 16% 45% 15%

Sample Statistics
KETOCONAZOLE

Characteristic N % % Basis
Plotted 72 96% Spiked
Estimated Values 29 39% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 75 .  
False Negatives 3 4% 3 out of 75
Not Spiked 40 .  
False Positives 0 0% 0 out of 40

BQS OBSP Determination:
LAMIVUDINE
METHOD: 2440 , TESTIDCODE: 68018LCM56
Open Data Set

Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 79% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 72% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 80 µl & ERA 0406-15-08: 80 µl Pct Recovery = 88% Analysis Date = 11/05/15 SpikeMix = ERA 0406-15-08: 80 µl & Abs 052215: 80 µl Pct Recovery = 82% Analysis Date = 11/24/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 79% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 80 µl & Abs 051315: 80 µl Pct Recovery = 67% Analysis Date = 11/18/16 SpikeMix = ERA 04281604: 80 µl & ERA 04281603: 80 µl Pct Recovery = 70% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & ERA 04281604: 80 µl Pct Recovery = 72% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 64% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 68% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 68% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 68% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 99% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 107% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-04: 15 µl & Abs 041814: 15 µl Pct Recovery = 131% Analysis Date = 12/06/14 SpikeMix = ERA 0318-14-02: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 82% Analysis Date = 10/25/14 SpikeMix = Abs 041614: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 125% Analysis Date = 10/11/14 SpikeMix = ERA 0318-14-02: 60 µl & ERA 0319-14-04: 60 µl Pct Recovery = 99% Analysis Date = 08/28/14 SpikeMix = ERA 0319-14-04: 60 µl & ERA 0319-14-05: 60 µl Pct Recovery = 79% Analysis Date = 05/07/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 13% Analysis Date = 03/11/15 SpikeMix = ERA 0318-14-02: 15 µl & Abs 041714: 15 µl Pct Recovery = 14% Analysis Date = 06/11/14 SpikeMix = Abs 041614: 60 µl & Abs 041714: 60 µl Pct Recovery = 7% Analysis Date = 05/21/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 48% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-08: 40 µl & Abs 052215: 40 µl Pct Recovery = 83% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 37% Analysis Date = 11/04/15 SpikeMix = ERA 0406-15-07A: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 71% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-08: 40 µl & ERA 0406-15-09: 40 µl Pct Recovery = 67% Analysis Date = 07/30/15 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 70% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 80% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 91% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 65% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 64% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 76% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 76% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 64% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 67% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 37% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 42% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 41% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 38% Analysis Date = 04/30/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 134% Analysis Date = 04/10/15 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 106% Analysis Date = 02/10/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 143% Analysis Date = 12/07/14 SpikeMix = ERA 0318-14-02: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 93% Analysis Date = 10/11/14 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 97% Analysis Date = 09/12/14 SpikeMix = Abs 041614: 30 µl & ERA 0319-14-04: 30 µl Pct Recovery = 94% Analysis Date = 08/16/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 74% Analysis Date = 07/13/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 69% Analysis Date = 10/10/14 SpikeMix = Abs 041714: 30 µl & Abs 041814: 30 µl Pct Recovery = 120% Analysis Date = 06/28/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 16% Analysis Date = 05/17/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 39% Analysis Date = 04/27/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 102% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-08: 20 µl & ERA 0406-15-09: 20 µl Pct Recovery = 68% Analysis Date = 11/25/15 SpikeMix = Abs 050115: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 52% Analysis Date = 09/10/15 SpikeMix = ERA 0406-15-08: 20 µl & Abs 052215: 20 µl Pct Recovery = 92% Analysis Date = 06/26/15 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 90% Analysis Date = 01/18/17 Pct Recovery = 70% Analysis Date = 01/14/17 Pct Recovery = 70% Analysis Date = 01/14/17 Pct Recovery = 70% Analysis Date = 01/09/17 Pct Recovery = 70% Analysis Date = 01/09/17 Pct Recovery = 70% Analysis Date = 01/04/17 Pct Recovery = 70% Analysis Date = 01/04/17 Pct Recovery = 70% Analysis Date = 12/30/16 Pct Recovery = 70% Analysis Date = 12/30/16 Pct Recovery = 70% Analysis Date = 12/25/16 Pct Recovery = 70% Analysis Date = 12/25/16 Pct Recovery = 70% Analysis Date = 12/20/16 Pct Recovery = 70% Analysis Date = 12/20/16 Pct Recovery = 70% Analysis Date = 12/15/16 Pct Recovery = 70% Analysis Date = 12/15/16 Pct Recovery = 70% Analysis Date = 12/10/16 Pct Recovery = 70% Analysis Date = 12/10/16 Pct Recovery = 70% Analysis Date = 12/05/16 Pct Recovery = 70% Analysis Date = 12/05/16 Pct Recovery = 70% Analysis Date = 12/01/16 Pct Recovery = 70% Analysis Date = 12/01/16 Pct Recovery = 70% Analysis Date = 11/26/16 Pct Recovery = 70% Analysis Date = 11/26/16 Pct Recovery = 70% Analysis Date = 11/21/16 Pct Recovery = 70% Analysis Date = 11/21/16 Pct Recovery = 70% Analysis Date = 11/16/16 Pct Recovery = 70% Analysis Date = 11/16/16 Pct Recovery = 70% Analysis Date = 11/11/16 Pct Recovery = 70% Analysis Date = 11/11/16 Pct Recovery = 70% Analysis Date = 11/06/16 Pct Recovery = 70% Analysis Date = 11/06/16 Pct Recovery = 70% Analysis Date = 11/01/16 Pct Recovery = 70% Analysis Date = 11/01/16 Pct Recovery = 70% Analysis Date = 10/27/16 Pct Recovery = 70% Analysis Date = 10/27/16 Pct Recovery = 70% Analysis Date = 10/22/16 Pct Recovery = 70% Analysis Date = 10/22/16 Pct Recovery = 70% Analysis Date = 10/18/16 Pct Recovery = 70% Analysis Date = 10/18/16 Pct Recovery = 70% Analysis Date = 10/13/16 Pct Recovery = 70% Analysis Date = 10/13/16 Pct Recovery = 70% Analysis Date = 10/08/16 Pct Recovery = 70% Analysis Date = 10/08/16 Pct Recovery = 70% Analysis Date = 10/03/16 Pct Recovery = 70% Analysis Date = 10/03/16 Pct Recovery = 70% Analysis Date = 09/28/16 Pct Recovery = 70% Analysis Date = 09/28/16 Pct Recovery = 70% Analysis Date = 09/23/16 Pct Recovery = 70% Analysis Date = 09/23/16 Pct Recovery = 70% Analysis Date = 09/18/16 Pct Recovery = 70% Analysis Date = 09/18/16 Pct Recovery = 70% Analysis Date = 09/13/16 Pct Recovery = 70% Analysis Date = 09/13/16 Pct Recovery = 70% Analysis Date = 09/08/16 Pct Recovery = 70% Analysis Date = 09/08/16 Pct Recovery = 70% Analysis Date = 09/04/16 Pct Recovery = 70% Analysis Date = 09/04/16 Pct Recovery = 70% Analysis Date = 08/30/16 Pct Recovery = 70% Analysis Date = 08/30/16 Pct Recovery = 70% Analysis Date = 08/25/16 Pct Recovery = 70% Analysis Date = 08/25/16 Pct Recovery = 70% Analysis Date = 08/20/16 Pct Recovery = 70% Analysis Date = 08/20/16 Pct Recovery = 70% Analysis Date = 08/15/16 Pct Recovery = 70% Analysis Date = 08/15/16 Pct Recovery = 70% Analysis Date = 08/10/16 Pct Recovery = 70% Analysis Date = 08/10/16 Pct Recovery = 70% Analysis Date = 08/05/16 Pct Recovery = 70% Analysis Date = 08/05/16 Pct Recovery = 70% Analysis Date = 07/31/16 Pct Recovery = 70% Analysis Date = 07/31/16 Pct Recovery = 70% Analysis Date = 07/26/16 Pct Recovery = 70% Analysis Date = 07/26/16 Pct Recovery = 70% Analysis Date = 07/22/16 Pct Recovery = 70% Analysis Date = 07/22/16 Pct Recovery = 70% Analysis Date = 07/17/16 Pct Recovery = 70% Analysis Date = 07/17/16 Pct Recovery = 70% Analysis Date = 07/12/16 Pct Recovery = 70% Analysis Date = 07/12/16 Pct Recovery = 70% Analysis Date = 07/07/16 Pct Recovery = 70% Analysis Date = 07/07/16 Pct Recovery = 70% Analysis Date = 07/02/16 Pct Recovery = 70% Analysis Date = 07/02/16 Pct Recovery = 70% Analysis Date = 06/27/16 Pct Recovery = 70% Analysis Date = 06/27/16 Pct Recovery = 70% Analysis Date = 06/22/16 Pct Recovery = 70% Analysis Date = 06/22/16 Pct Recovery = 70% Analysis Date = 06/17/16 Pct Recovery = 70% Analysis Date = 06/17/16 Pct Recovery = 70% Analysis Date = 06/12/16 Pct Recovery = 70% Analysis Date = 06/12/16 Pct Recovery = 70% Analysis Date = 06/08/16 Pct Recovery = 70% Analysis Date = 06/08/16 Pct Recovery = 70% Analysis Date = 06/03/16 Pct Recovery = 70% Analysis Date = 06/03/16 Pct Recovery = 70% Analysis Date = 05/29/16 Pct Recovery = 70% Analysis Date = 05/29/16 Pct Recovery = 70% Analysis Date = 05/24/16 Pct Recovery = 71% Analysis Date = 05/24/16 Pct Recovery = 71% Analysis Date = 05/19/16 Pct Recovery = 71% Analysis Date = 05/19/16 Pct Recovery = 71% Analysis Date = 05/14/16 Pct Recovery = 71% Analysis Date = 05/14/16 Pct Recovery = 71% Analysis Date = 05/09/16 Pct Recovery = 71% Analysis Date = 05/09/16 Pct Recovery = 71% Analysis Date = 05/04/16 Pct Recovery = 71% Analysis Date = 05/04/16 Pct Recovery = 71% Analysis Date = 04/29/16 Pct Recovery = 71% Analysis Date = 04/29/16 Pct Recovery = 71% Analysis Date = 04/25/16 Pct Recovery = 71% Analysis Date = 04/25/16 Pct Recovery = 71% Analysis Date = 04/20/16 Pct Recovery = 71% Analysis Date = 04/20/16 Pct Recovery = 71% Analysis Date = 04/15/16 Pct Recovery = 71% Analysis Date = 04/15/16 Pct Recovery = 71% Analysis Date = 04/10/16 Pct Recovery = 71% Analysis Date = 04/10/16 Pct Recovery = 71% Analysis Date = 04/05/16 Pct Recovery = 71% Analysis Date = 04/05/16 Pct Recovery = 71% Analysis Date = 03/31/16 Pct Recovery = 71% Analysis Date = 03/31/16 Pct Recovery = 71% Analysis Date = 03/26/16 Pct Recovery = 71% Analysis Date = 03/26/16 Pct Recovery = 71% Analysis Date = 03/21/16 Pct Recovery = 71% Analysis Date = 03/21/16 Pct Recovery = 71% Analysis Date = 03/16/16 Pct Recovery = 71% Analysis Date = 03/16/16 Pct Recovery = 71% Analysis Date = 03/12/16 Pct Recovery = 71% Analysis Date = 03/12/16 Pct Recovery = 71% Analysis Date = 03/07/16 Pct Recovery = 71% Analysis Date = 03/07/16 Pct Recovery = 71% Analysis Date = 03/02/16 Pct Recovery = 72% Analysis Date = 03/02/16 Pct Recovery = 72% Analysis Date = 02/26/16 Pct Recovery = 72% Analysis Date = 02/26/16 Pct Recovery = 72% Analysis Date = 02/21/16 Pct Recovery = 72% Analysis Date = 02/21/16 Pct Recovery = 72% Analysis Date = 02/16/16 Pct Recovery = 72% Analysis Date = 02/16/16 Pct Recovery = 72% Analysis Date = 02/11/16 Pct Recovery = 72% Analysis Date = 02/11/16 Pct Recovery = 72% Analysis Date = 02/06/16 Pct Recovery = 72% Analysis Date = 02/06/16 Pct Recovery = 72% Analysis Date = 02/01/16 Pct Recovery = 72% Analysis Date = 02/01/16 Pct Recovery = 72% Analysis Date = 01/28/16 Pct Recovery = 72% Analysis Date = 01/28/16 Pct Recovery = 72% Analysis Date = 01/23/16 Pct Recovery = 73% Analysis Date = 01/23/16 Pct Recovery = 73% Analysis Date = 01/18/16 Pct Recovery = 73% Analysis Date = 01/18/16 Pct Recovery = 73% Analysis Date = 01/13/16 Pct Recovery = 73% Analysis Date = 01/13/16 Pct Recovery = 73% Analysis Date = 01/08/16 Pct Recovery = 73% Analysis Date = 01/08/16 Pct Recovery = 73% Analysis Date = 01/03/16 Pct Recovery = 73% Analysis Date = 01/03/16 Pct Recovery = 73% Analysis Date = 12/29/15 Pct Recovery = 73% Analysis Date = 12/29/15 Pct Recovery = 73% Analysis Date = 12/24/15 Pct Recovery = 73% Analysis Date = 12/24/15 Pct Recovery = 73% Analysis Date = 12/19/15 Pct Recovery = 74% Analysis Date = 12/19/15 Pct Recovery = 74% Analysis Date = 12/15/15 Pct Recovery = 74% Analysis Date = 12/15/15 Pct Recovery = 74% Analysis Date = 12/10/15 Pct Recovery = 74% Analysis Date = 12/10/15 Pct Recovery = 74% Analysis Date = 12/05/15 Pct Recovery = 74% Analysis Date = 12/05/15 Pct Recovery = 74% Analysis Date = 11/30/15 Pct Recovery = 74% Analysis Date = 11/30/15 Pct Recovery = 74% Analysis Date = 11/25/15 Pct Recovery = 74% Analysis Date = 11/25/15 Pct Recovery = 74% Analysis Date = 11/20/15 Pct Recovery = 74% Analysis Date = 11/20/15 Pct Recovery = 74% Analysis Date = 11/15/15 Pct Recovery = 75% Analysis Date = 11/15/15 Pct Recovery = 75% Analysis Date = 11/10/15 Pct Recovery = 75% Analysis Date = 11/10/15 Pct Recovery = 75% Analysis Date = 11/05/15 Pct Recovery = 75% Analysis Date = 11/05/15 Pct Recovery = 75% Analysis Date = 11/01/15 Pct Recovery = 75% Analysis Date = 11/01/15 Pct Recovery = 75% Analysis Date = 10/27/15 Pct Recovery = 75% Analysis Date = 10/27/15 Pct Recovery = 75% Analysis Date = 10/22/15 Pct Recovery = 76% Analysis Date = 10/22/15 Pct Recovery = 76% Analysis Date = 10/17/15 Pct Recovery = 76% Analysis Date = 10/17/15 Pct Recovery = 76% Analysis Date = 10/12/15 Pct Recovery = 76% Analysis Date = 10/12/15 Pct Recovery = 76% Analysis Date = 10/07/15 Pct Recovery = 76% Analysis Date = 10/07/15 Pct Recovery = 76% Analysis Date = 10/02/15 Pct Recovery = 76% Analysis Date = 10/02/15 Pct Recovery = 76% Analysis Date = 09/27/15 Pct Recovery = 77% Analysis Date = 09/27/15 Pct Recovery = 77% Analysis Date = 09/22/15 Pct Recovery = 77% Analysis Date = 09/22/15 Pct Recovery = 77% Analysis Date = 09/17/15 Pct Recovery = 77% Analysis Date = 09/17/15 Pct Recovery = 77% Analysis Date = 09/13/15 Pct Recovery = 78% Analysis Date = 09/13/15 Pct Recovery = 78% Analysis Date = 09/08/15 Pct Recovery = 78% Analysis Date = 09/08/15 Pct Recovery = 78% Analysis Date = 09/03/15 Pct Recovery = 78% Analysis Date = 09/03/15 Pct Recovery = 78% Analysis Date = 08/29/15 Pct Recovery = 78% Analysis Date = 08/29/15 Pct Recovery = 78% Analysis Date = 08/24/15 Pct Recovery = 79% Analysis Date = 08/24/15 Pct Recovery = 79% Analysis Date = 08/19/15 Pct Recovery = 79% Analysis Date = 08/19/15 Pct Recovery = 79% Analysis Date = 08/14/15 Pct Recovery = 79% Analysis Date = 08/14/15 Pct Recovery = 79% Analysis Date = 08/09/15 Pct Recovery = 80% Analysis Date = 08/09/15 Pct Recovery = 80% Analysis Date = 08/04/15 Pct Recovery = 80% Analysis Date = 08/04/15 Pct Recovery = 80% Analysis Date = 07/31/15 Pct Recovery = 80% Analysis Date = 07/31/15 Pct Recovery = 80% Analysis Date = 07/26/15 Pct Recovery = 81% Analysis Date = 07/26/15 Pct Recovery = 81% Analysis Date = 07/21/15 Pct Recovery = 81% Analysis Date = 07/21/15 Pct Recovery = 81% Analysis Date = 07/16/15 Pct Recovery = 81% Analysis Date = 07/16/15 Pct Recovery = 81% Analysis Date = 07/11/15 Pct Recovery = 81% Analysis Date = 07/11/15 Pct Recovery = 81% Analysis Date = 07/06/15 Pct Recovery = 82% Analysis Date = 07/06/15 Pct Recovery = 82% Analysis Date = 07/01/15 Pct Recovery = 82% Analysis Date = 07/01/15 Pct Recovery = 82% Analysis Date = 06/26/15 Pct Recovery = 82% Analysis Date = 06/26/15 Pct Recovery = 82% Analysis Date = 06/21/15 Pct Recovery = 83% Analysis Date = 06/21/15 Pct Recovery = 83% Analysis Date = 06/17/15 Pct Recovery = 83% Analysis Date = 06/17/15 Pct Recovery = 83% Analysis Date = 06/12/15 Pct Recovery = 83% Analysis Date = 06/12/15 Pct Recovery = 83% Analysis Date = 06/07/15 Pct Recovery = 84% Analysis Date = 06/07/15 Pct Recovery = 84% Analysis Date = 06/02/15 Pct Recovery = 84% Analysis Date = 06/02/15 Pct Recovery = 84% Analysis Date = 05/28/15 Pct Recovery = 84% Analysis Date = 05/28/15 Pct Recovery = 84% Analysis Date = 05/23/15 Pct Recovery = 84% Analysis Date = 05/23/15 Pct Recovery = 84% Analysis Date = 05/18/15 Pct Recovery = 85% Analysis Date = 05/18/15 Pct Recovery = 85% Analysis Date = 05/13/15 Pct Recovery = 85% Analysis Date = 05/13/15 Pct Recovery = 85% Analysis Date = 05/08/15 Pct Recovery = 85% Analysis Date = 05/08/15 Pct Recovery = 85% Analysis Date = 05/04/15 Pct Recovery = 86% Analysis Date = 05/04/15 Pct Recovery = 86% Analysis Date = 04/29/15 Pct Recovery = 86% Analysis Date = 04/29/15 Pct Recovery = 86% Analysis Date = 04/24/15 Pct Recovery = 86% Analysis Date = 04/24/15 Pct Recovery = 86% Analysis Date = 04/19/15 Pct Recovery = 87% Analysis Date = 04/19/15 Pct Recovery = 87% Analysis Date = 04/14/15 Pct Recovery = 87% Analysis Date = 04/14/15 Pct Recovery = 87% Analysis Date = 04/09/15 Pct Recovery = 87% Analysis Date = 04/09/15 Pct Recovery = 87% Analysis Date = 04/04/15 Pct Recovery = 87% Analysis Date = 04/04/15 Pct Recovery = 87% Analysis Date = 03/30/15 Pct Recovery = 87% Analysis Date = 03/30/15 Pct Recovery = 87% Analysis Date = 03/25/15 Pct Recovery = 86% Analysis Date = 03/25/15 Pct Recovery = 86% Analysis Date = 03/21/15 Pct Recovery = 86% Analysis Date = 03/21/15 Pct Recovery = 86% Analysis Date = 03/16/15 Pct Recovery = 86% Analysis Date = 03/16/15 Pct Recovery = 86% Analysis Date = 03/11/15 Pct Recovery = 85% Analysis Date = 03/11/15 Pct Recovery = 85% Analysis Date = 03/06/15 Pct Recovery = 85% Analysis Date = 03/06/15 Pct Recovery = 85% Analysis Date = 03/01/15 Pct Recovery = 85% Analysis Date = 03/01/15 Pct Recovery = 85% Analysis Date = 02/24/15 Pct Recovery = 85% Analysis Date = 02/24/15 Pct Recovery = 85% Analysis Date = 02/19/15 Pct Recovery = 84% Analysis Date = 02/19/15 Pct Recovery = 84% Analysis Date = 02/14/15 Pct Recovery = 84% Analysis Date = 02/14/15 Pct Recovery = 84% Analysis Date = 02/09/15 Pct Recovery = 84% Analysis Date = 02/09/15 Pct Recovery = 84% Analysis Date = 02/05/15 Pct Recovery = 83% Analysis Date = 02/05/15 Pct Recovery = 83% Analysis Date = 01/31/15 Pct Recovery = 83% Analysis Date = 01/31/15 Pct Recovery = 83% Analysis Date = 01/26/15 Pct Recovery = 83% Analysis Date = 01/26/15 Pct Recovery = 83% Analysis Date = 01/21/15 Pct Recovery = 83% Analysis Date = 01/21/15 Pct Recovery = 83% Analysis Date = 01/16/15 Pct Recovery = 82% Analysis Date = 01/16/15 Pct Recovery = 82% Analysis Date = 01/11/15 Pct Recovery = 82% Analysis Date = 01/11/15 Pct Recovery = 82% Analysis Date = 01/06/15 Pct Recovery = 82% Analysis Date = 01/06/15 Pct Recovery = 82% Analysis Date = 01/01/15 Pct Recovery = 81% Analysis Date = 01/01/15 Pct Recovery = 81% Analysis Date = 12/27/14 Pct Recovery = 81% Analysis Date = 12/27/14 Pct Recovery = 81% Analysis Date = 12/23/14 Pct Recovery = 81% Analysis Date = 12/23/14 Pct Recovery = 81% Analysis Date = 12/18/14 Pct Recovery = 81% Analysis Date = 12/18/14 Pct Recovery = 81% Analysis Date = 12/13/14 Pct Recovery = 80% Analysis Date = 12/13/14 Pct Recovery = 80% Analysis Date = 12/08/14 Pct Recovery = 80% Analysis Date = 12/08/14 Pct Recovery = 80% Analysis Date = 12/03/14 Pct Recovery = 80% Analysis Date = 12/03/14 Pct Recovery = 80% Analysis Date = 11/28/14 Pct Recovery = 79% Analysis Date = 11/28/14 Pct Recovery = 79% Analysis Date = 11/23/14 Pct Recovery = 79% Analysis Date = 11/23/14 Pct Recovery = 79% Analysis Date = 11/18/14 Pct Recovery = 79% Analysis Date = 11/18/14 Pct Recovery = 79% Analysis Date = 11/13/14 Pct Recovery = 78% Analysis Date = 11/13/14 Pct Recovery = 78% Analysis Date = 11/09/14 Pct Recovery = 78% Analysis Date = 11/09/14 Pct Recovery = 78% Analysis Date = 11/04/14 Pct Recovery = 77% Analysis Date = 11/04/14 Pct Recovery = 77% Analysis Date = 10/30/14 Pct Recovery = 77% Analysis Date = 10/30/14 Pct Recovery = 77% Analysis Date = 10/25/14 Pct Recovery = 77% Analysis Date = 10/25/14 Pct Recovery = 77% Analysis Date = 10/20/14 Pct Recovery = 76% Analysis Date = 10/20/14 Pct Recovery = 76% Analysis Date = 10/15/14 Pct Recovery = 76% Analysis Date = 10/15/14 Pct Recovery = 76% Analysis Date = 10/10/14 Pct Recovery = 76% Analysis Date = 10/10/14 Pct Recovery = 76% Analysis Date = 10/05/14 Pct Recovery = 75% Analysis Date = 10/05/14 Pct Recovery = 75% Analysis Date = 09/30/14 Pct Recovery = 75% Analysis Date = 09/30/14 Pct Recovery = 75% Analysis Date = 09/26/14 Pct Recovery = 74% Analysis Date = 09/26/14 Pct Recovery = 74% Analysis Date = 09/21/14 Pct Recovery = 74% Analysis Date = 09/21/14 Pct Recovery = 74% Analysis Date = 09/16/14 Pct Recovery = 74% Analysis Date = 09/16/14 Pct Recovery = 74% Analysis Date = 09/11/14 Pct Recovery = 73% Analysis Date = 09/11/14 Pct Recovery = 73% Analysis Date = 09/06/14 Pct Recovery = 73% Analysis Date = 09/06/14 Pct Recovery = 73% Analysis Date = 09/01/14 Pct Recovery = 72% Analysis Date = 09/01/14 Pct Recovery = 72% Analysis Date = 08/27/14 Pct Recovery = 72% Analysis Date = 08/27/14 Pct Recovery = 72% Analysis Date = 08/22/14 Pct Recovery = 72% Analysis Date = 08/22/14 Pct Recovery = 72% Analysis Date = 08/17/14 Pct Recovery = 71% Analysis Date = 08/17/14 Pct Recovery = 71% Analysis Date = 08/13/14 Pct Recovery = 71% Analysis Date = 08/13/14 Pct Recovery = 71% Analysis Date = 08/08/14 Pct Recovery = 70% Analysis Date = 08/08/14 Pct Recovery = 70% Analysis Date = 08/03/14 Pct Recovery = 70% Analysis Date = 08/03/14 Pct Recovery = 70% Analysis Date = 07/29/14 Pct Recovery = 69% Analysis Date = 07/29/14 Pct Recovery = 69% Analysis Date = 07/24/14 Pct Recovery = 69% Analysis Date = 07/24/14 Pct Recovery = 69% Analysis Date = 07/19/14 Pct Recovery = 68% Analysis Date = 07/19/14 Pct Recovery = 68% Analysis Date = 07/14/14 Pct Recovery = 68% Analysis Date = 07/14/14 Pct Recovery = 68% Analysis Date = 07/09/14 Pct Recovery = 67% Analysis Date = 07/09/14 Pct Recovery = 67% Analysis Date = 07/04/14 Pct Recovery = 67% Analysis Date = 07/04/14 Pct Recovery = 67% Analysis Date = 06/30/14 Pct Recovery = 66% Analysis Date = 06/30/14 Pct Recovery = 66% Analysis Date = 06/25/14 Pct Recovery = 66% Analysis Date = 06/25/14 Pct Recovery = 66% Analysis Date = 06/20/14 Pct Recovery = 65% Analysis Date = 06/20/14 Pct Recovery = 65% Analysis Date = 06/15/14 Pct Recovery = 65% Analysis Date = 06/15/14 Pct Recovery = 65% Analysis Date = 06/10/14 Pct Recovery = 64% Analysis Date = 06/10/14 Pct Recovery = 64% Analysis Date = 06/05/14 Pct Recovery = 64% Analysis Date = 06/05/14 Pct Recovery = 64% Analysis Date = 05/31/14 Pct Recovery = 63% Analysis Date = 05/31/14 Pct Recovery = 63% Analysis Date = 05/26/14 Pct Recovery = 63% Analysis Date = 05/26/14 Pct Recovery = 63% Analysis Date = 05/21/14 Pct Recovery = 62% Analysis Date = 05/21/14 Pct Recovery = 62% Analysis Date = 05/17/14 Pct Recovery = 62% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
LAMIVUDINE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 56 74% 29% 72% 21%
Total 56 74% 29% 72% 21%

Sample Statistics
LAMIVUDINE

Characteristic N % % Basis
Plotted 56 74% Spiked
Estimated Values 18 24% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 3 4% Spiked
Spiked 76 .  
False Negatives 17 22% 17 out of 76
Not Spiked 39 .  
False Positives 0 0% 0 out of 39

BQS OBSP Determination:
LIDOCAINE
METHOD: 2440 , TESTIDCODE: 67462LCM56
Open Data Set

Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 84% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 83% Analysis Date = 11/05/15 SpikeMix = ERA 0406-15-08: 80 µl & Abs 052215: 80 µl Pct Recovery = 89% Analysis Date = 11/04/15 SpikeMix = Abs 052215: 80 µl & Abs 050115: 80 µl Pct Recovery = 89% Analysis Date = 01/17/16 SpikeMix = ERA 0406-15-09: 80 µl & ERA 0406-15-07A: 80 µl Pct Recovery = 81% Analysis Date = 11/24/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 81% Analysis Date = 10/01/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 83% Analysis Date = 09/24/16 SpikeMix = Crescent EN160610015: 80 µl & Abs 061416: 80 µl Pct Recovery = 87% Analysis Date = 09/24/16 SpikeMix = Abs 061416: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 82% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 102% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 108% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 101% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 100% Analysis Date = 11/18/16 SpikeMix = ERA 04281604: 80 µl & ERA 04281603: 80 µl Pct Recovery = 84% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & ERA 04281604: 80 µl Pct Recovery = 82% Analysis Date = 04/29/15 SpikeMix = ERA 0319-14-05: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 105% Analysis Date = 03/11/15 SpikeMix = ERA 0318-14-02: 15 µl & Abs 041714: 15 µl Pct Recovery = 88% Analysis Date = 02/06/15 SpikeMix = Abs 041814: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 85% Analysis Date = 12/06/14 SpikeMix = ERA 0318-14-02: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 90% Analysis Date = 08/21/14 SpikeMix = ERA 0318-14-02: 60 µl & Abs 041714: 60 µl Pct Recovery = 67% Analysis Date = 07/26/14 SpikeMix = ERA 0319-14-05: 60 µl & ERA 0318-14-02: 60 µl Pct Recovery = 85% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 75% Analysis Date = 12/07/14 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 106% Analysis Date = 10/25/14 SpikeMix = Abs 041614: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 144% Analysis Date = 06/22/14 SpikeMix = Abs 041814: 60 µl & Abs 041614: 60 µl Pct Recovery = 88% Analysis Date = 06/11/14 SpikeMix = Abs 041614: 60 µl & Abs 041714: 60 µl Pct Recovery = 88% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-08: 40 µl & Abs 052215: 40 µl Pct Recovery = 84% Analysis Date = 02/23/16 SpikeMix = Abs 052215: 40 µl & Abs 050115: 40 µl Pct Recovery = 89% Analysis Date = 09/10/15 SpikeMix = Abs 052215: 40 µl & ERA 0406-15-07A: 40 µl Pct Recovery = 92% Analysis Date = 07/31/15 SpikeMix = Abs 051315: 40 µl & Abs 052215: 40 µl Pct Recovery = 73% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-08: 40 µl & ERA 0406-15-09: 40 µl Pct Recovery = 78% Analysis Date = 07/31/15 SpikeMix = ERA 0406-15-09: 40 µl & Abs 050115: 40 µl Pct Recovery = 90% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 83% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 72% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 77% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 81% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 69% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 79% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 76% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 78% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 83% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 82% Analysis Date = 12/07/14 SpikeMix = ERA 0318-14-02: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 94% Analysis Date = 04/30/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 97% Analysis Date = 02/10/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 86% Analysis Date = 08/30/14 SpikeMix = ERA 0318-14-02: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 76% Analysis Date = 07/20/14 SpikeMix = ERA 0318-14-02: 30 µl & Abs 041714: 30 µl Pct Recovery = 65% Analysis Date = 09/12/14 SpikeMix = Abs 041614: 30 µl & ERA 0319-14-04: 30 µl Pct Recovery = 67% Analysis Date = 07/13/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 78% Analysis Date = 06/28/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 72% Analysis Date = 05/30/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 83% Analysis Date = 05/17/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 84% Analysis Date = 04/23/14 SpikeMix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.2: 20 µl Pct Recovery = 74% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 68% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 64% Analysis Date = 02/23/16 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 81% Analysis Date = 11/24/15 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 89% Analysis Date = 09/09/15 SpikeMix = ERA 0406-15-08: 20 µl & Abs 052215: 20 µl Pct Recovery = 85% Analysis Date = 08/27/15 SpikeMix = Abs 052215: 20 µl & Abs 050115: 20 µl Pct Recovery = 91% Analysis Date = 07/09/15 SpikeMix = Abs 050115: 20 µl & Abs 052215: 20 µl Pct Recovery = 75% Analysis Date = 06/26/15 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 82% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 74% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 90% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-08: 20 µl & ERA 0406-15-09: 20 µl Pct Recovery = 77% Analysis Date = 11/24/15 SpikeMix = ERA 0406-15-09: 20 µl & Abs 050115: 20 µl Pct Recovery = 79% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-09: 20 µl Pct Recovery = 65% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 113% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 121% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 96% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 94% Analysis Date = 04/09/16 SpikeMix = Abs 051315: 10 µl & ERA 0406-15-09: 10 µl Pct Recovery = 73% Analysis Date = 04/09/16 SpikeMix = Abs 051315: 10 µl & ERA 0406-15-09: 10 µl Pct Recovery = 90% Analysis Date = 01/04/17 Pct Recovery = 92% Analysis Date = 12/31/16 Pct Recovery = 91% Analysis Date = 12/31/16 Pct Recovery = 91% Analysis Date = 12/26/16 Pct Recovery = 91% Analysis Date = 12/26/16 Pct Recovery = 91% Analysis Date = 12/21/16 Pct Recovery = 91% Analysis Date = 12/21/16 Pct Recovery = 91% Analysis Date = 12/16/16 Pct Recovery = 91% Analysis Date = 12/16/16 Pct Recovery = 91% Analysis Date = 12/11/16 Pct Recovery = 91% Analysis Date = 12/11/16 Pct Recovery = 91% Analysis Date = 12/06/16 Pct Recovery = 90% Analysis Date = 12/06/16 Pct Recovery = 90% Analysis Date = 12/01/16 Pct Recovery = 90% Analysis Date = 12/01/16 Pct Recovery = 90% Analysis Date = 11/26/16 Pct Recovery = 90% Analysis Date = 11/26/16 Pct Recovery = 90% Analysis Date = 11/21/16 Pct Recovery = 90% Analysis Date = 11/21/16 Pct Recovery = 90% Analysis Date = 11/16/16 Pct Recovery = 90% Analysis Date = 11/16/16 Pct Recovery = 90% Analysis Date = 11/11/16 Pct Recovery = 89% Analysis Date = 11/11/16 Pct Recovery = 89% Analysis Date = 11/06/16 Pct Recovery = 89% Analysis Date = 11/06/16 Pct Recovery = 89% Analysis Date = 11/01/16 Pct Recovery = 89% Analysis Date = 11/01/16 Pct Recovery = 89% Analysis Date = 10/27/16 Pct Recovery = 89% Analysis Date = 10/27/16 Pct Recovery = 89% Analysis Date = 10/22/16 Pct Recovery = 88% Analysis Date = 10/22/16 Pct Recovery = 88% Analysis Date = 10/17/16 Pct Recovery = 88% Analysis Date = 10/17/16 Pct Recovery = 88% Analysis Date = 10/13/16 Pct Recovery = 88% Analysis Date = 10/13/16 Pct Recovery = 88% Analysis Date = 10/08/16 Pct Recovery = 88% Analysis Date = 10/08/16 Pct Recovery = 88% Analysis Date = 10/03/16 Pct Recovery = 88% Analysis Date = 10/03/16 Pct Recovery = 88% Analysis Date = 09/28/16 Pct Recovery = 87% Analysis Date = 09/28/16 Pct Recovery = 87% Analysis Date = 09/23/16 Pct Recovery = 87% Analysis Date = 09/23/16 Pct Recovery = 87% Analysis Date = 09/18/16 Pct Recovery = 87% Analysis Date = 09/18/16 Pct Recovery = 87% Analysis Date = 09/13/16 Pct Recovery = 87% Analysis Date = 09/13/16 Pct Recovery = 87% Analysis Date = 09/08/16 Pct Recovery = 87% Analysis Date = 09/08/16 Pct Recovery = 87% Analysis Date = 09/03/16 Pct Recovery = 86% Analysis Date = 09/03/16 Pct Recovery = 86% Analysis Date = 08/29/16 Pct Recovery = 86% Analysis Date = 08/29/16 Pct Recovery = 86% Analysis Date = 08/24/16 Pct Recovery = 86% Analysis Date = 08/24/16 Pct Recovery = 86% Analysis Date = 08/19/16 Pct Recovery = 86% Analysis Date = 08/19/16 Pct Recovery = 86% Analysis Date = 08/14/16 Pct Recovery = 86% Analysis Date = 08/14/16 Pct Recovery = 86% Analysis Date = 08/09/16 Pct Recovery = 85% Analysis Date = 08/09/16 Pct Recovery = 85% Analysis Date = 08/04/16 Pct Recovery = 85% Analysis Date = 08/04/16 Pct Recovery = 85% Analysis Date = 07/30/16 Pct Recovery = 85% Analysis Date = 07/30/16 Pct Recovery = 85% Analysis Date = 07/25/16 Pct Recovery = 85% Analysis Date = 07/25/16 Pct Recovery = 85% Analysis Date = 07/21/16 Pct Recovery = 85% Analysis Date = 07/21/16 Pct Recovery = 85% Analysis Date = 07/16/16 Pct Recovery = 85% Analysis Date = 07/16/16 Pct Recovery = 85% Analysis Date = 07/11/16 Pct Recovery = 85% Analysis Date = 07/11/16 Pct Recovery = 85% Analysis Date = 07/06/16 Pct Recovery = 84% Analysis Date = 07/06/16 Pct Recovery = 84% Analysis Date = 07/01/16 Pct Recovery = 84% Analysis Date = 07/01/16 Pct Recovery = 84% Analysis Date = 06/26/16 Pct Recovery = 84% Analysis Date = 06/26/16 Pct Recovery = 84% Analysis Date = 06/21/16 Pct Recovery = 84% Analysis Date = 06/21/16 Pct Recovery = 84% Analysis Date = 06/16/16 Pct Recovery = 84% Analysis Date = 06/16/16 Pct Recovery = 84% Analysis Date = 06/11/16 Pct Recovery = 84% Analysis Date = 06/11/16 Pct Recovery = 84% Analysis Date = 06/06/16 Pct Recovery = 84% Analysis Date = 06/06/16 Pct Recovery = 84% Analysis Date = 06/01/16 Pct Recovery = 84% Analysis Date = 06/01/16 Pct Recovery = 84% Analysis Date = 05/27/16 Pct Recovery = 84% Analysis Date = 05/27/16 Pct Recovery = 84% Analysis Date = 05/22/16 Pct Recovery = 84% Analysis Date = 05/22/16 Pct Recovery = 84% Analysis Date = 05/17/16 Pct Recovery = 84% Analysis Date = 05/17/16 Pct Recovery = 84% Analysis Date = 05/12/16 Pct Recovery = 84% Analysis Date = 05/12/16 Pct Recovery = 84% Analysis Date = 05/07/16 Pct Recovery = 84% Analysis Date = 05/07/16 Pct Recovery = 84% Analysis Date = 05/02/16 Pct Recovery = 84% Analysis Date = 05/02/16 Pct Recovery = 84% Analysis Date = 04/28/16 Pct Recovery = 83% Analysis Date = 04/28/16 Pct Recovery = 83% Analysis Date = 04/23/16 Pct Recovery = 83% Analysis Date = 04/23/16 Pct Recovery = 83% Analysis Date = 04/18/16 Pct Recovery = 83% Analysis Date = 04/18/16 Pct Recovery = 83% Analysis Date = 04/13/16 Pct Recovery = 83% Analysis Date = 04/13/16 Pct Recovery = 83% Analysis Date = 04/08/16 Pct Recovery = 83% Analysis Date = 04/08/16 Pct Recovery = 83% Analysis Date = 04/03/16 Pct Recovery = 83% Analysis Date = 04/03/16 Pct Recovery = 83% Analysis Date = 03/29/16 Pct Recovery = 83% Analysis Date = 03/29/16 Pct Recovery = 83% Analysis Date = 03/24/16 Pct Recovery = 83% Analysis Date = 03/24/16 Pct Recovery = 83% Analysis Date = 03/19/16 Pct Recovery = 83% Analysis Date = 03/19/16 Pct Recovery = 83% Analysis Date = 03/14/16 Pct Recovery = 83% Analysis Date = 03/14/16 Pct Recovery = 83% Analysis Date = 03/09/16 Pct Recovery = 83% Analysis Date = 03/09/16 Pct Recovery = 83% Analysis Date = 03/04/16 Pct Recovery = 83% Analysis Date = 03/04/16 Pct Recovery = 83% Analysis Date = 02/28/16 Pct Recovery = 83% Analysis Date = 02/28/16 Pct Recovery = 83% Analysis Date = 02/23/16 Pct Recovery = 83% Analysis Date = 02/23/16 Pct Recovery = 83% Analysis Date = 02/18/16 Pct Recovery = 83% Analysis Date = 02/18/16 Pct Recovery = 83% Analysis Date = 02/13/16 Pct Recovery = 83% Analysis Date = 02/13/16 Pct Recovery = 83% Analysis Date = 02/09/16 Pct Recovery = 83% Analysis Date = 02/09/16 Pct Recovery = 83% Analysis Date = 02/04/16 Pct Recovery = 83% Analysis Date = 02/04/16 Pct Recovery = 83% Analysis Date = 01/30/16 Pct Recovery = 83% Analysis Date = 01/30/16 Pct Recovery = 83% Analysis Date = 01/25/16 Pct Recovery = 83% Analysis Date = 01/25/16 Pct Recovery = 83% Analysis Date = 01/20/16 Pct Recovery = 83% Analysis Date = 01/20/16 Pct Recovery = 83% Analysis Date = 01/15/16 Pct Recovery = 83% Analysis Date = 01/15/16 Pct Recovery = 83% Analysis Date = 01/10/16 Pct Recovery = 83% Analysis Date = 01/10/16 Pct Recovery = 83% Analysis Date = 01/05/16 Pct Recovery = 83% Analysis Date = 01/05/16 Pct Recovery = 83% Analysis Date = 12/31/15 Pct Recovery = 83% Analysis Date = 12/31/15 Pct Recovery = 83% Analysis Date = 12/26/15 Pct Recovery = 83% Analysis Date = 12/26/15 Pct Recovery = 83% Analysis Date = 12/21/15 Pct Recovery = 83% Analysis Date = 12/21/15 Pct Recovery = 83% Analysis Date = 12/16/15 Pct Recovery = 83% Analysis Date = 12/16/15 Pct Recovery = 83% Analysis Date = 12/11/15 Pct Recovery = 83% Analysis Date = 12/11/15 Pct Recovery = 83% Analysis Date = 12/06/15 Pct Recovery = 83% Analysis Date = 12/06/15 Pct Recovery = 83% Analysis Date = 12/01/15 Pct Recovery = 83% Analysis Date = 12/01/15 Pct Recovery = 83% Analysis Date = 11/26/15 Pct Recovery = 83% Analysis Date = 11/26/15 Pct Recovery = 83% Analysis Date = 11/21/15 Pct Recovery = 83% Analysis Date = 11/21/15 Pct Recovery = 83% Analysis Date = 11/17/15 Pct Recovery = 83% Analysis Date = 11/17/15 Pct Recovery = 83% Analysis Date = 11/12/15 Pct Recovery = 83% Analysis Date = 11/12/15 Pct Recovery = 83% Analysis Date = 11/07/15 Pct Recovery = 83% Analysis Date = 11/07/15 Pct Recovery = 83% Analysis Date = 11/02/15 Pct Recovery = 83% Analysis Date = 11/02/15 Pct Recovery = 83% Analysis Date = 10/28/15 Pct Recovery = 83% Analysis Date = 10/28/15 Pct Recovery = 83% Analysis Date = 10/23/15 Pct Recovery = 83% Analysis Date = 10/23/15 Pct Recovery = 83% Analysis Date = 10/18/15 Pct Recovery = 83% Analysis Date = 10/18/15 Pct Recovery = 83% Analysis Date = 10/13/15 Pct Recovery = 83% Analysis Date = 10/13/15 Pct Recovery = 83% Analysis Date = 10/08/15 Pct Recovery = 84% Analysis Date = 10/08/15 Pct Recovery = 84% Analysis Date = 10/03/15 Pct Recovery = 84% Analysis Date = 10/03/15 Pct Recovery = 84% Analysis Date = 09/28/15 Pct Recovery = 84% Analysis Date = 09/28/15 Pct Recovery = 84% Analysis Date = 09/23/15 Pct Recovery = 84% Analysis Date = 09/23/15 Pct Recovery = 84% Analysis Date = 09/18/15 Pct Recovery = 84% Analysis Date = 09/18/15 Pct Recovery = 84% Analysis Date = 09/13/15 Pct Recovery = 84% Analysis Date = 09/13/15 Pct Recovery = 84% Analysis Date = 09/08/15 Pct Recovery = 84% Analysis Date = 09/08/15 Pct Recovery = 84% Analysis Date = 09/03/15 Pct Recovery = 84% Analysis Date = 09/03/15 Pct Recovery = 84% Analysis Date = 08/29/15 Pct Recovery = 85% Analysis Date = 08/29/15 Pct Recovery = 85% Analysis Date = 08/25/15 Pct Recovery = 85% Analysis Date = 08/25/15 Pct Recovery = 85% Analysis Date = 08/20/15 Pct Recovery = 85% Analysis Date = 08/20/15 Pct Recovery = 85% Analysis Date = 08/15/15 Pct Recovery = 85% Analysis Date = 08/15/15 Pct Recovery = 85% Analysis Date = 08/10/15 Pct Recovery = 85% Analysis Date = 08/10/15 Pct Recovery = 85% Analysis Date = 08/05/15 Pct Recovery = 85% Analysis Date = 08/05/15 Pct Recovery = 85% Analysis Date = 07/31/15 Pct Recovery = 86% Analysis Date = 07/31/15 Pct Recovery = 86% Analysis Date = 07/26/15 Pct Recovery = 86% Analysis Date = 07/26/15 Pct Recovery = 86% Analysis Date = 07/21/15 Pct Recovery = 86% Analysis Date = 07/21/15 Pct Recovery = 86% Analysis Date = 07/16/15 Pct Recovery = 86% Analysis Date = 07/16/15 Pct Recovery = 86% Analysis Date = 07/11/15 Pct Recovery = 86% Analysis Date = 07/11/15 Pct Recovery = 86% Analysis Date = 07/06/15 Pct Recovery = 86% Analysis Date = 07/06/15 Pct Recovery = 86% Analysis Date = 07/01/15 Pct Recovery = 87% Analysis Date = 07/01/15 Pct Recovery = 87% Analysis Date = 06/26/15 Pct Recovery = 87% Analysis Date = 06/26/15 Pct Recovery = 87% Analysis Date = 06/21/15 Pct Recovery = 87% Analysis Date = 06/21/15 Pct Recovery = 87% Analysis Date = 06/16/15 Pct Recovery = 87% Analysis Date = 06/16/15 Pct Recovery = 87% Analysis Date = 06/11/15 Pct Recovery = 87% Analysis Date = 06/11/15 Pct Recovery = 87% Analysis Date = 06/07/15 Pct Recovery = 87% Analysis Date = 06/07/15 Pct Recovery = 87% Analysis Date = 06/02/15 Pct Recovery = 87% Analysis Date = 06/02/15 Pct Recovery = 87% Analysis Date = 05/28/15 Pct Recovery = 87% Analysis Date = 05/28/15 Pct Recovery = 87% Analysis Date = 05/23/15 Pct Recovery = 87% Analysis Date = 05/23/15 Pct Recovery = 87% Analysis Date = 05/18/15 Pct Recovery = 87% Analysis Date = 05/18/15 Pct Recovery = 87% Analysis Date = 05/13/15 Pct Recovery = 87% Analysis Date = 05/13/15 Pct Recovery = 87% Analysis Date = 05/08/15 Pct Recovery = 87% Analysis Date = 05/08/15 Pct Recovery = 87% Analysis Date = 05/03/15 Pct Recovery = 87% Analysis Date = 05/03/15 Pct Recovery = 87% Analysis Date = 04/28/15 Pct Recovery = 87% Analysis Date = 04/28/15 Pct Recovery = 87% Analysis Date = 04/23/15 Pct Recovery = 87% Analysis Date = 04/23/15 Pct Recovery = 87% Analysis Date = 04/18/15 Pct Recovery = 87% Analysis Date = 04/18/15 Pct Recovery = 87% Analysis Date = 04/13/15 Pct Recovery = 87% Analysis Date = 04/13/15 Pct Recovery = 87% Analysis Date = 04/08/15 Pct Recovery = 87% Analysis Date = 04/08/15 Pct Recovery = 87% Analysis Date = 04/03/15 Pct Recovery = 87% Analysis Date = 04/03/15 Pct Recovery = 87% Analysis Date = 03/29/15 Pct Recovery = 86% Analysis Date = 03/29/15 Pct Recovery = 86% Analysis Date = 03/24/15 Pct Recovery = 86% Analysis Date = 03/24/15 Pct Recovery = 86% Analysis Date = 03/19/15 Pct Recovery = 86% Analysis Date = 03/19/15 Pct Recovery = 86% Analysis Date = 03/15/15 Pct Recovery = 86% Analysis Date = 03/15/15 Pct Recovery = 86% Analysis Date = 03/10/15 Pct Recovery = 86% Analysis Date = 03/10/15 Pct Recovery = 86% Analysis Date = 03/05/15 Pct Recovery = 86% Analysis Date = 03/05/15 Pct Recovery = 86% Analysis Date = 02/28/15 Pct Recovery = 86% Analysis Date = 02/28/15 Pct Recovery = 86% Analysis Date = 02/23/15 Pct Recovery = 86% Analysis Date = 02/23/15 Pct Recovery = 86% Analysis Date = 02/18/15 Pct Recovery = 86% Analysis Date = 02/18/15 Pct Recovery = 86% Analysis Date = 02/13/15 Pct Recovery = 86% Analysis Date = 02/13/15 Pct Recovery = 86% Analysis Date = 02/08/15 Pct Recovery = 86% Analysis Date = 02/08/15 Pct Recovery = 86% Analysis Date = 02/03/15 Pct Recovery = 86% Analysis Date = 02/03/15 Pct Recovery = 86% Analysis Date = 01/29/15 Pct Recovery = 86% Analysis Date = 01/29/15 Pct Recovery = 86% Analysis Date = 01/24/15 Pct Recovery = 86% Analysis Date = 01/24/15 Pct Recovery = 86% Analysis Date = 01/19/15 Pct Recovery = 86% Analysis Date = 01/19/15 Pct Recovery = 86% Analysis Date = 01/14/15 Pct Recovery = 86% Analysis Date = 01/14/15 Pct Recovery = 86% Analysis Date = 01/09/15 Pct Recovery = 86% Analysis Date = 01/09/15 Pct Recovery = 86% Analysis Date = 01/04/15 Pct Recovery = 86% Analysis Date = 01/04/15 Pct Recovery = 86% Analysis Date = 12/30/14 Pct Recovery = 86% Analysis Date = 12/30/14 Pct Recovery = 86% Analysis Date = 12/25/14 Pct Recovery = 86% Analysis Date = 12/25/14 Pct Recovery = 86% Analysis Date = 12/21/14 Pct Recovery = 86% Analysis Date = 12/21/14 Pct Recovery = 86% Analysis Date = 12/16/14 Pct Recovery = 85% Analysis Date = 12/16/14 Pct Recovery = 85% Analysis Date = 12/11/14 Pct Recovery = 85% Analysis Date = 12/11/14 Pct Recovery = 85% Analysis Date = 12/06/14 Pct Recovery = 85% Analysis Date = 12/06/14 Pct Recovery = 85% Analysis Date = 12/01/14 Pct Recovery = 85% Analysis Date = 12/01/14 Pct Recovery = 85% Analysis Date = 11/26/14 Pct Recovery = 85% Analysis Date = 11/26/14 Pct Recovery = 85% Analysis Date = 11/21/14 Pct Recovery = 85% Analysis Date = 11/21/14 Pct Recovery = 85% Analysis Date = 11/16/14 Pct Recovery = 85% Analysis Date = 11/16/14 Pct Recovery = 85% Analysis Date = 11/11/14 Pct Recovery = 85% Analysis Date = 11/11/14 Pct Recovery = 85% Analysis Date = 11/06/14 Pct Recovery = 85% Analysis Date = 11/06/14 Pct Recovery = 85% Analysis Date = 11/01/14 Pct Recovery = 85% Analysis Date = 11/01/14 Pct Recovery = 85% Analysis Date = 10/27/14 Pct Recovery = 85% Analysis Date = 10/27/14 Pct Recovery = 85% Analysis Date = 10/22/14 Pct Recovery = 85% Analysis Date = 10/22/14 Pct Recovery = 85% Analysis Date = 10/17/14 Pct Recovery = 85% Analysis Date = 10/17/14 Pct Recovery = 85% Analysis Date = 10/12/14 Pct Recovery = 84% Analysis Date = 10/12/14 Pct Recovery = 84% Analysis Date = 10/07/14 Pct Recovery = 84% Analysis Date = 10/07/14 Pct Recovery = 84% Analysis Date = 10/03/14 Pct Recovery = 84% Analysis Date = 10/03/14 Pct Recovery = 84% Analysis Date = 09/28/14 Pct Recovery = 84% Analysis Date = 09/28/14 Pct Recovery = 84% Analysis Date = 09/23/14 Pct Recovery = 84% Analysis Date = 09/23/14 Pct Recovery = 84% Analysis Date = 09/18/14 Pct Recovery = 84% Analysis Date = 09/18/14 Pct Recovery = 84% Analysis Date = 09/13/14 Pct Recovery = 84% Analysis Date = 09/13/14 Pct Recovery = 84% Analysis Date = 09/08/14 Pct Recovery = 84% Analysis Date = 09/08/14 Pct Recovery = 84% Analysis Date = 09/03/14 Pct Recovery = 84% Analysis Date = 09/03/14 Pct Recovery = 84% Analysis Date = 08/29/14 Pct Recovery = 84% Analysis Date = 08/29/14 Pct Recovery = 84% Analysis Date = 08/24/14 Pct Recovery = 84% Analysis Date = 08/24/14 Pct Recovery = 84% Analysis Date = 08/19/14 Pct Recovery = 84% Analysis Date = 08/19/14 Pct Recovery = 84% Analysis Date = 08/14/14 Pct Recovery = 84% Analysis Date = 08/14/14 Pct Recovery = 84% Analysis Date = 08/09/14 Pct Recovery = 84% Analysis Date = 08/09/14 Pct Recovery = 84% Analysis Date = 08/04/14 Pct Recovery = 83% Analysis Date = 08/04/14 Pct Recovery = 83% Analysis Date = 07/30/14 Pct Recovery = 83% Analysis Date = 07/30/14 Pct Recovery = 83% Analysis Date = 07/25/14 Pct Recovery = 83% Analysis Date = 07/25/14 Pct Recovery = 83% Analysis Date = 07/20/14 Pct Recovery = 83% Analysis Date = 07/20/14 Pct Recovery = 83% Analysis Date = 07/15/14 Pct Recovery = 83% Analysis Date = 07/15/14 Pct Recovery = 83% Analysis Date = 07/11/14 Pct Recovery = 83% Analysis Date = 07/11/14 Pct Recovery = 83% Analysis Date = 07/06/14 Pct Recovery = 83% Analysis Date = 07/06/14 Pct Recovery = 83% Analysis Date = 07/01/14 Pct Recovery = 83% Analysis Date = 07/01/14 Pct Recovery = 83% Analysis Date = 06/26/14 Pct Recovery = 83% Analysis Date = 06/26/14 Pct Recovery = 83% Analysis Date = 06/21/14 Pct Recovery = 83% Analysis Date = 06/21/14 Pct Recovery = 83% Analysis Date = 06/16/14 Pct Recovery = 83% Analysis Date = 06/16/14 Pct Recovery = 83% Analysis Date = 06/11/14 Pct Recovery = 82% Analysis Date = 06/11/14 Pct Recovery = 82% Analysis Date = 06/06/14 Pct Recovery = 82% Analysis Date = 06/06/14 Pct Recovery = 82% Analysis Date = 06/01/14 Pct Recovery = 82% Analysis Date = 06/01/14 Pct Recovery = 82% Analysis Date = 05/27/14 Pct Recovery = 82% Analysis Date = 05/27/14 Pct Recovery = 82% Analysis Date = 05/22/14 Pct Recovery = 82% Analysis Date = 05/22/14 Pct Recovery = 82% Analysis Date = 05/17/14 Pct Recovery = 82% Analysis Date = 05/17/14 Pct Recovery = 82% Analysis Date = 05/12/14 Pct Recovery = 82% Analysis Date = 05/12/14 Pct Recovery = 82% Analysis Date = 05/07/14 Pct Recovery = 82% Analysis Date = 05/07/14 Pct Recovery = 82% Analysis Date = 05/02/14 Pct Recovery = 81% Analysis Date = 05/02/14 Pct Recovery = 81% Analysis Date = 04/27/14 Pct Recovery = 81% Analysis Date = 04/27/14 Pct Recovery = 81% Analysis Date = 04/23/14 Pct Recovery = 81% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
LIDOCAINE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 6 98% 17% 95% 17%
>= Reporting Level 66 84% 12% 83% 9%
Total 72 85% 13% 83% 10%

Sample Statistics
LIDOCAINE

Characteristic N % % Basis
Plotted 72 95% Spiked
Estimated Values 4 5% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 4 5% Spiked
Spiked 76 .  
False Negatives 0 0% 0 out of 76
Not Spiked 39 .  
False Positives 1 3% 1 out of 39

BQS OBSP Determination:
LOPERAMIDE
METHOD: 2440 , TESTIDCODE: 67515LCM56
Open Data Set

Analysis Date = 01/17/16 SpikeMix = ERA 0406-15-09: 80 µl & ERA 0406-15-07A: 80 µl Pct Recovery = 58% Analysis Date = 11/24/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 66% Analysis Date = 11/05/15 SpikeMix = ERA 0406-15-08: 80 µl & Abs 052215: 80 µl Pct Recovery = 46% Analysis Date = 11/04/15 SpikeMix = Abs 052215: 80 µl & Abs 050115: 80 µl Pct Recovery = 43% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 51% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 54% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 77% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 67% Analysis Date = 04/29/15 SpikeMix = ERA 0319-14-05: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 53% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 38% Analysis Date = 01/16/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 42% Analysis Date = 12/07/14 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 41% Analysis Date = 12/06/14 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 33% Analysis Date = 08/28/14 SpikeMix = ERA 0319-14-04: 60 µl & ERA 0319-14-05: 60 µl Pct Recovery = 38% Analysis Date = 07/26/14 SpikeMix = ERA 0319-14-05: 60 µl & ERA 0318-14-02: 60 µl Pct Recovery = 47% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-08: 40 µl & Abs 052215: 40 µl Pct Recovery = 63% Analysis Date = 02/23/16 SpikeMix = Abs 052215: 40 µl & Abs 050115: 40 µl Pct Recovery = 64% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 56% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 61% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 21% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 35% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 20% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 34% Analysis Date = 11/04/14 SpikeMix = Abs 041714: 8 µl & ERA 0319-14-05: 8 µl Pct Recovery = 11% Analysis Date = 10/24/14 SpikeMix = ERA 0319-14-05: 8 µl & Abs 041614: 8 µl Pct Recovery = 30% Analysis Date = 08/30/14 SpikeMix = ERA 0318-14-02: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 47% Analysis Date = 08/16/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 24% Analysis Date = 07/13/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 17% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 37% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 45% Analysis Date = 11/18/16 SpikeMix = ERA 04281604: 80 µl & ERA 04281603: 80 µl Pct Recovery = 46% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & ERA 04281604: 80 µl Pct Recovery = 39% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 45% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 41% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 69% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 85% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 69% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 67% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 42% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 50% Analysis Date = 01/18/17 Pct Recovery = 54% Analysis Date = 01/14/17 Pct Recovery = 54% Analysis Date = 01/14/17 Pct Recovery = 54% Analysis Date = 01/09/17 Pct Recovery = 53% Analysis Date = 01/09/17 Pct Recovery = 53% Analysis Date = 01/05/17 Pct Recovery = 53% Analysis Date = 01/05/17 Pct Recovery = 53% Analysis Date = 12/31/16 Pct Recovery = 53% Analysis Date = 12/31/16 Pct Recovery = 53% Analysis Date = 12/26/16 Pct Recovery = 53% Analysis Date = 12/26/16 Pct Recovery = 53% Analysis Date = 12/22/16 Pct Recovery = 53% Analysis Date = 12/22/16 Pct Recovery = 53% Analysis Date = 12/17/16 Pct Recovery = 52% Analysis Date = 12/17/16 Pct Recovery = 52% Analysis Date = 12/13/16 Pct Recovery = 52% Analysis Date = 12/13/16 Pct Recovery = 52% Analysis Date = 12/08/16 Pct Recovery = 52% Analysis Date = 12/08/16 Pct Recovery = 52% Analysis Date = 12/03/16 Pct Recovery = 52% Analysis Date = 12/03/16 Pct Recovery = 52% Analysis Date = 11/29/16 Pct Recovery = 52% Analysis Date = 11/29/16 Pct Recovery = 52% Analysis Date = 11/24/16 Pct Recovery = 51% Analysis Date = 11/24/16 Pct Recovery = 51% Analysis Date = 11/20/16 Pct Recovery = 51% Analysis Date = 11/20/16 Pct Recovery = 51% Analysis Date = 11/15/16 Pct Recovery = 51% Analysis Date = 11/15/16 Pct Recovery = 51% Analysis Date = 11/10/16 Pct Recovery = 51% Analysis Date = 11/10/16 Pct Recovery = 51% Analysis Date = 11/06/16 Pct Recovery = 51% Analysis Date = 11/06/16 Pct Recovery = 51% Analysis Date = 11/01/16 Pct Recovery = 51% Analysis Date = 11/01/16 Pct Recovery = 51% Analysis Date = 10/28/16 Pct Recovery = 50% Analysis Date = 10/28/16 Pct Recovery = 50% Analysis Date = 10/23/16 Pct Recovery = 50% Analysis Date = 10/23/16 Pct Recovery = 50% Analysis Date = 10/18/16 Pct Recovery = 50% Analysis Date = 10/18/16 Pct Recovery = 50% Analysis Date = 10/14/16 Pct Recovery = 50% Analysis Date = 10/14/16 Pct Recovery = 50% Analysis Date = 10/09/16 Pct Recovery = 50% Analysis Date = 10/09/16 Pct Recovery = 50% Analysis Date = 10/05/16 Pct Recovery = 50% Analysis Date = 10/05/16 Pct Recovery = 50% Analysis Date = 09/30/16 Pct Recovery = 50% Analysis Date = 09/30/16 Pct Recovery = 50% Analysis Date = 09/25/16 Pct Recovery = 49% Analysis Date = 09/25/16 Pct Recovery = 49% Analysis Date = 09/21/16 Pct Recovery = 49% Analysis Date = 09/21/16 Pct Recovery = 49% Analysis Date = 09/16/16 Pct Recovery = 49% Analysis Date = 09/16/16 Pct Recovery = 49% Analysis Date = 09/12/16 Pct Recovery = 49% Analysis Date = 09/12/16 Pct Recovery = 49% Analysis Date = 09/07/16 Pct Recovery = 49% Analysis Date = 09/07/16 Pct Recovery = 49% Analysis Date = 09/02/16 Pct Recovery = 50% Analysis Date = 09/02/16 Pct Recovery = 50% Analysis Date = 08/29/16 Pct Recovery = 50% Analysis Date = 08/29/16 Pct Recovery = 50% Analysis Date = 08/24/16 Pct Recovery = 50% Analysis Date = 08/24/16 Pct Recovery = 50% Analysis Date = 08/20/16 Pct Recovery = 50% Analysis Date = 08/20/16 Pct Recovery = 50% Analysis Date = 08/15/16 Pct Recovery = 51% Analysis Date = 08/15/16 Pct Recovery = 51% Analysis Date = 08/10/16 Pct Recovery = 51% Analysis Date = 08/10/16 Pct Recovery = 51% Analysis Date = 08/06/16 Pct Recovery = 51% Analysis Date = 08/06/16 Pct Recovery = 51% Analysis Date = 08/01/16 Pct Recovery = 52% Analysis Date = 08/01/16 Pct Recovery = 52% Analysis Date = 07/28/16 Pct Recovery = 52% Analysis Date = 07/28/16 Pct Recovery = 52% Analysis Date = 07/23/16 Pct Recovery = 52% Analysis Date = 07/23/16 Pct Recovery = 52% Analysis Date = 07/18/16 Pct Recovery = 52% Analysis Date = 07/18/16 Pct Recovery = 52% Analysis Date = 07/14/16 Pct Recovery = 52% Analysis Date = 07/14/16 Pct Recovery = 52% Analysis Date = 07/09/16 Pct Recovery = 52% Analysis Date = 07/09/16 Pct Recovery = 52% Analysis Date = 07/04/16 Pct Recovery = 53% Analysis Date = 07/04/16 Pct Recovery = 53% Analysis Date = 06/30/16 Pct Recovery = 53% Analysis Date = 06/30/16 Pct Recovery = 53% Analysis Date = 06/25/16 Pct Recovery = 53% Analysis Date = 06/25/16 Pct Recovery = 53% Analysis Date = 06/21/16 Pct Recovery = 53% Analysis Date = 06/21/16 Pct Recovery = 53% Analysis Date = 06/16/16 Pct Recovery = 53% Analysis Date = 06/16/16 Pct Recovery = 53% Analysis Date = 06/11/16 Pct Recovery = 53% Analysis Date = 06/11/16 Pct Recovery = 53% Analysis Date = 06/07/16 Pct Recovery = 53% Analysis Date = 06/07/16 Pct Recovery = 53% Analysis Date = 06/02/16 Pct Recovery = 53% Analysis Date = 06/02/16 Pct Recovery = 53% Analysis Date = 05/29/16 Pct Recovery = 54% Analysis Date = 05/29/16 Pct Recovery = 54% Analysis Date = 05/24/16 Pct Recovery = 54% Analysis Date = 05/24/16 Pct Recovery = 54% Analysis Date = 05/19/16 Pct Recovery = 54% Analysis Date = 05/19/16 Pct Recovery = 54% Analysis Date = 05/15/16 Pct Recovery = 54% Analysis Date = 05/15/16 Pct Recovery = 54% Analysis Date = 05/10/16 Pct Recovery = 54% Analysis Date = 05/10/16 Pct Recovery = 54% Analysis Date = 05/06/16 Pct Recovery = 54% Analysis Date = 05/06/16 Pct Recovery = 54% Analysis Date = 05/01/16 Pct Recovery = 54% Analysis Date = 05/01/16 Pct Recovery = 54% Analysis Date = 04/26/16 Pct Recovery = 54% Analysis Date = 04/26/16 Pct Recovery = 54% Analysis Date = 04/22/16 Pct Recovery = 55% Analysis Date = 04/22/16 Pct Recovery = 55% Analysis Date = 04/17/16 Pct Recovery = 55% Analysis Date = 04/17/16 Pct Recovery = 55% Analysis Date = 04/13/16 Pct Recovery = 55% Analysis Date = 04/13/16 Pct Recovery = 55% Analysis Date = 04/08/16 Pct Recovery = 55% Analysis Date = 04/08/16 Pct Recovery = 55% Analysis Date = 04/03/16 Pct Recovery = 55% Analysis Date = 04/03/16 Pct Recovery = 55% Analysis Date = 03/30/16 Pct Recovery = 55% Analysis Date = 03/30/16 Pct Recovery = 55% Analysis Date = 03/25/16 Pct Recovery = 55% Analysis Date = 03/25/16 Pct Recovery = 55% Analysis Date = 03/21/16 Pct Recovery = 55% Analysis Date = 03/21/16 Pct Recovery = 55% Analysis Date = 03/16/16 Pct Recovery = 56% Analysis Date = 03/16/16 Pct Recovery = 56% Analysis Date = 03/11/16 Pct Recovery = 56% Analysis Date = 03/11/16 Pct Recovery = 56% Analysis Date = 03/07/16 Pct Recovery = 56% Analysis Date = 03/07/16 Pct Recovery = 56% Analysis Date = 03/02/16 Pct Recovery = 56% Analysis Date = 03/02/16 Pct Recovery = 56% Analysis Date = 02/27/16 Pct Recovery = 56% Analysis Date = 02/27/16 Pct Recovery = 56% Analysis Date = 02/22/16 Pct Recovery = 56% Analysis Date = 02/22/16 Pct Recovery = 56% Analysis Date = 02/17/16 Pct Recovery = 56% Analysis Date = 02/17/16 Pct Recovery = 56% Analysis Date = 02/13/16 Pct Recovery = 56% Analysis Date = 02/13/16 Pct Recovery = 56% Analysis Date = 02/08/16 Pct Recovery = 56% Analysis Date = 02/08/16 Pct Recovery = 56% Analysis Date = 02/04/16 Pct Recovery = 55% Analysis Date = 02/04/16 Pct Recovery = 55% Analysis Date = 01/30/16 Pct Recovery = 55% Analysis Date = 01/30/16 Pct Recovery = 55% Analysis Date = 01/25/16 Pct Recovery = 55% Analysis Date = 01/25/16 Pct Recovery = 55% Analysis Date = 01/21/16 Pct Recovery = 55% Analysis Date = 01/21/16 Pct Recovery = 55% Analysis Date = 01/16/16 Pct Recovery = 55% Analysis Date = 01/16/16 Pct Recovery = 55% Analysis Date = 01/11/16 Pct Recovery = 55% Analysis Date = 01/11/16 Pct Recovery = 55% Analysis Date = 01/07/16 Pct Recovery = 55% Analysis Date = 01/07/16 Pct Recovery = 55% Analysis Date = 01/02/16 Pct Recovery = 55% Analysis Date = 01/02/16 Pct Recovery = 55% Analysis Date = 12/29/15 Pct Recovery = 55% Analysis Date = 12/29/15 Pct Recovery = 55% Analysis Date = 12/24/15 Pct Recovery = 55% Analysis Date = 12/24/15 Pct Recovery = 55% Analysis Date = 12/19/15 Pct Recovery = 55% Analysis Date = 12/19/15 Pct Recovery = 55% Analysis Date = 12/15/15 Pct Recovery = 55% Analysis Date = 12/15/15 Pct Recovery = 55% Analysis Date = 12/10/15 Pct Recovery = 55% Analysis Date = 12/10/15 Pct Recovery = 55% Analysis Date = 12/06/15 Pct Recovery = 55% Analysis Date = 12/06/15 Pct Recovery = 55% Analysis Date = 12/01/15 Pct Recovery = 55% Analysis Date = 12/01/15 Pct Recovery = 55% Analysis Date = 11/26/15 Pct Recovery = 55% Analysis Date = 11/26/15 Pct Recovery = 55% Analysis Date = 11/22/15 Pct Recovery = 54% Analysis Date = 11/22/15 Pct Recovery = 54% Analysis Date = 11/17/15 Pct Recovery = 54% Analysis Date = 11/17/15 Pct Recovery = 54% Analysis Date = 11/13/15 Pct Recovery = 54% Analysis Date = 11/13/15 Pct Recovery = 54% Analysis Date = 11/08/15 Pct Recovery = 54% Analysis Date = 11/08/15 Pct Recovery = 54% Analysis Date = 11/03/15 Pct Recovery = 54% Analysis Date = 11/03/15 Pct Recovery = 54% Analysis Date = 10/30/15 Pct Recovery = 54% Analysis Date = 10/30/15 Pct Recovery = 54% Analysis Date = 10/25/15 Pct Recovery = 53% Analysis Date = 10/25/15 Pct Recovery = 53% Analysis Date = 10/21/15 Pct Recovery = 53% Analysis Date = 10/21/15 Pct Recovery = 53% Analysis Date = 10/16/15 Pct Recovery = 53% Analysis Date = 10/16/15 Pct Recovery = 53% Analysis Date = 10/11/15 Pct Recovery = 53% Analysis Date = 10/11/15 Pct Recovery = 53% Analysis Date = 10/07/15 Pct Recovery = 52% Analysis Date = 10/07/15 Pct Recovery = 52% Analysis Date = 10/02/15 Pct Recovery = 52% Analysis Date = 10/02/15 Pct Recovery = 52% Analysis Date = 09/28/15 Pct Recovery = 52% Analysis Date = 09/28/15 Pct Recovery = 52% Analysis Date = 09/23/15 Pct Recovery = 52% Analysis Date = 09/23/15 Pct Recovery = 52% Analysis Date = 09/18/15 Pct Recovery = 51% Analysis Date = 09/18/15 Pct Recovery = 51% Analysis Date = 09/14/15 Pct Recovery = 51% Analysis Date = 09/14/15 Pct Recovery = 51% Analysis Date = 09/09/15 Pct Recovery = 51% Analysis Date = 09/09/15 Pct Recovery = 51% Analysis Date = 09/05/15 Pct Recovery = 51% Analysis Date = 09/05/15 Pct Recovery = 51% Analysis Date = 08/31/15 Pct Recovery = 50% Analysis Date = 08/31/15 Pct Recovery = 50% Analysis Date = 08/26/15 Pct Recovery = 50% Analysis Date = 08/26/15 Pct Recovery = 50% Analysis Date = 08/22/15 Pct Recovery = 50% Analysis Date = 08/22/15 Pct Recovery = 50% Analysis Date = 08/17/15 Pct Recovery = 50% Analysis Date = 08/17/15 Pct Recovery = 50% Analysis Date = 08/13/15 Pct Recovery = 50% Analysis Date = 08/13/15 Pct Recovery = 50% Analysis Date = 08/08/15 Pct Recovery = 49% Analysis Date = 08/08/15 Pct Recovery = 49% Analysis Date = 08/03/15 Pct Recovery = 49% Analysis Date = 08/03/15 Pct Recovery = 49% Analysis Date = 07/30/15 Pct Recovery = 49% Analysis Date = 07/30/15 Pct Recovery = 49% Analysis Date = 07/25/15 Pct Recovery = 49% Analysis Date = 07/25/15 Pct Recovery = 49% Analysis Date = 07/21/15 Pct Recovery = 48% Analysis Date = 07/21/15 Pct Recovery = 48% Analysis Date = 07/16/15 Pct Recovery = 48% Analysis Date = 07/16/15 Pct Recovery = 48% Analysis Date = 07/11/15 Pct Recovery = 48% Analysis Date = 07/11/15 Pct Recovery = 48% Analysis Date = 07/07/15 Pct Recovery = 48% Analysis Date = 07/07/15 Pct Recovery = 48% Analysis Date = 07/02/15 Pct Recovery = 47% Analysis Date = 07/02/15 Pct Recovery = 47% Analysis Date = 06/27/15 Pct Recovery = 47% Analysis Date = 06/27/15 Pct Recovery = 47% Analysis Date = 06/23/15 Pct Recovery = 47% Analysis Date = 06/23/15 Pct Recovery = 47% Analysis Date = 06/18/15 Pct Recovery = 47% Analysis Date = 06/18/15 Pct Recovery = 47% Analysis Date = 06/14/15 Pct Recovery = 46% Analysis Date = 06/14/15 Pct Recovery = 46% Analysis Date = 06/09/15 Pct Recovery = 46% Analysis Date = 06/09/15 Pct Recovery = 46% Analysis Date = 06/04/15 Pct Recovery = 46% Analysis Date = 06/04/15 Pct Recovery = 46% Analysis Date = 05/31/15 Pct Recovery = 46% Analysis Date = 05/31/15 Pct Recovery = 46% Analysis Date = 05/26/15 Pct Recovery = 45% Analysis Date = 05/26/15 Pct Recovery = 45% Analysis Date = 05/22/15 Pct Recovery = 45% Analysis Date = 05/22/15 Pct Recovery = 45% Analysis Date = 05/17/15 Pct Recovery = 45% Analysis Date = 05/17/15 Pct Recovery = 45% Analysis Date = 05/12/15 Pct Recovery = 45% Analysis Date = 05/12/15 Pct Recovery = 45% Analysis Date = 05/08/15 Pct Recovery = 44% Analysis Date = 05/08/15 Pct Recovery = 44% Analysis Date = 05/03/15 Pct Recovery = 44% Analysis Date = 05/03/15 Pct Recovery = 44% Analysis Date = 04/29/15 Pct Recovery = 44% Analysis Date = 04/29/15 Pct Recovery = 44% Analysis Date = 04/24/15 Pct Recovery = 44% Analysis Date = 04/24/15 Pct Recovery = 44% Analysis Date = 04/19/15 Pct Recovery = 44% Analysis Date = 04/19/15 Pct Recovery = 44% Analysis Date = 04/15/15 Pct Recovery = 43% Analysis Date = 04/15/15 Pct Recovery = 43% Analysis Date = 04/10/15 Pct Recovery = 43% Analysis Date = 04/10/15 Pct Recovery = 43% Analysis Date = 04/06/15 Pct Recovery = 43% Analysis Date = 04/06/15 Pct Recovery = 43% Analysis Date = 04/01/15 Pct Recovery = 43% Analysis Date = 04/01/15 Pct Recovery = 43% Analysis Date = 03/27/15 Pct Recovery = 42% Analysis Date = 03/27/15 Pct Recovery = 42% Analysis Date = 03/23/15 Pct Recovery = 42% Analysis Date = 03/23/15 Pct Recovery = 42% Analysis Date = 03/18/15 Pct Recovery = 42% Analysis Date = 03/18/15 Pct Recovery = 42% Analysis Date = 03/14/15 Pct Recovery = 42% Analysis Date = 03/14/15 Pct Recovery = 42% Analysis Date = 03/09/15 Pct Recovery = 41% Analysis Date = 03/09/15 Pct Recovery = 41% Analysis Date = 03/04/15 Pct Recovery = 41% Analysis Date = 03/04/15 Pct Recovery = 41% Analysis Date = 02/28/15 Pct Recovery = 41% Analysis Date = 02/28/15 Pct Recovery = 41% Analysis Date = 02/23/15 Pct Recovery = 41% Analysis Date = 02/23/15 Pct Recovery = 41% Analysis Date = 02/19/15 Pct Recovery = 40% Analysis Date = 02/19/15 Pct Recovery = 40% Analysis Date = 02/14/15 Pct Recovery = 40% Analysis Date = 02/14/15 Pct Recovery = 40% Analysis Date = 02/09/15 Pct Recovery = 40% Analysis Date = 02/09/15 Pct Recovery = 40% Analysis Date = 02/05/15 Pct Recovery = 40% Analysis Date = 02/05/15 Pct Recovery = 40% Analysis Date = 01/31/15 Pct Recovery = 39% Analysis Date = 01/31/15 Pct Recovery = 39% Analysis Date = 01/27/15 Pct Recovery = 39% Analysis Date = 01/27/15 Pct Recovery = 39% Analysis Date = 01/22/15 Pct Recovery = 39% Analysis Date = 01/22/15 Pct Recovery = 39% Analysis Date = 01/17/15 Pct Recovery = 39% Analysis Date = 01/17/15 Pct Recovery = 39% Analysis Date = 01/13/15 Pct Recovery = 38% Analysis Date = 01/13/15 Pct Recovery = 38% Analysis Date = 01/08/15 Pct Recovery = 38% Analysis Date = 01/08/15 Pct Recovery = 38% Analysis Date = 01/03/15 Pct Recovery = 38% Analysis Date = 01/03/15 Pct Recovery = 38% Analysis Date = 12/30/14 Pct Recovery = 38% Analysis Date = 12/30/14 Pct Recovery = 38% Analysis Date = 12/25/14 Pct Recovery = 38% Analysis Date = 12/25/14 Pct Recovery = 38% Analysis Date = 12/21/14 Pct Recovery = 37% Analysis Date = 12/21/14 Pct Recovery = 37% Analysis Date = 12/16/14 Pct Recovery = 37% Analysis Date = 12/16/14 Pct Recovery = 37% Analysis Date = 12/11/14 Pct Recovery = 37% Analysis Date = 12/11/14 Pct Recovery = 37% Analysis Date = 12/07/14 Pct Recovery = 37% Analysis Date = 12/07/14 Pct Recovery = 37% Analysis Date = 12/02/14 Pct Recovery = 36% Analysis Date = 12/02/14 Pct Recovery = 36% Analysis Date = 11/28/14 Pct Recovery = 36% Analysis Date = 11/28/14 Pct Recovery = 36% Analysis Date = 11/23/14 Pct Recovery = 36% Analysis Date = 11/23/14 Pct Recovery = 36% Analysis Date = 11/18/14 Pct Recovery = 36% Analysis Date = 11/18/14 Pct Recovery = 36% Analysis Date = 11/14/14 Pct Recovery = 35% Analysis Date = 11/14/14 Pct Recovery = 35% Analysis Date = 11/09/14 Pct Recovery = 35% Analysis Date = 11/09/14 Pct Recovery = 35% Analysis Date = 11/05/14 Pct Recovery = 35% Analysis Date = 11/05/14 Pct Recovery = 35% Analysis Date = 10/31/14 Pct Recovery = 35% Analysis Date = 10/31/14 Pct Recovery = 35% Analysis Date = 10/26/14 Pct Recovery = 35% Analysis Date = 10/26/14 Pct Recovery = 35% Analysis Date = 10/22/14 Pct Recovery = 34% Analysis Date = 10/22/14 Pct Recovery = 34% Analysis Date = 10/17/14 Pct Recovery = 34% Analysis Date = 10/17/14 Pct Recovery = 34% Analysis Date = 10/13/14 Pct Recovery = 34% Analysis Date = 10/13/14 Pct Recovery = 34% Analysis Date = 10/08/14 Pct Recovery = 34% Analysis Date = 10/08/14 Pct Recovery = 34% Analysis Date = 10/03/14 Pct Recovery = 33% Analysis Date = 10/03/14 Pct Recovery = 33% Analysis Date = 09/29/14 Pct Recovery = 33% Analysis Date = 09/29/14 Pct Recovery = 33% Analysis Date = 09/24/14 Pct Recovery = 33% Analysis Date = 09/24/14 Pct Recovery = 33% Analysis Date = 09/20/14 Pct Recovery = 33% Analysis Date = 09/20/14 Pct Recovery = 33% Analysis Date = 09/15/14 Pct Recovery = 32% Analysis Date = 09/15/14 Pct Recovery = 32% Analysis Date = 09/10/14 Pct Recovery = 32% Analysis Date = 09/10/14 Pct Recovery = 32% Analysis Date = 09/06/14 Pct Recovery = 32% Analysis Date = 09/06/14 Pct Recovery = 32% Analysis Date = 09/01/14 Pct Recovery = 32% Analysis Date = 09/01/14 Pct Recovery = 32% Analysis Date = 08/28/14 Pct Recovery = 31% Analysis Date = 08/28/14 Pct Recovery = 31% Analysis Date = 08/23/14 Pct Recovery = 31% Analysis Date = 08/23/14 Pct Recovery = 31% Analysis Date = 08/18/14 Pct Recovery = 31% Analysis Date = 08/18/14 Pct Recovery = 31% Analysis Date = 08/14/14 Pct Recovery = 31% Analysis Date = 08/14/14 Pct Recovery = 31% Analysis Date = 08/09/14 Pct Recovery = 31% Analysis Date = 08/09/14 Pct Recovery = 31% Analysis Date = 08/05/14 Pct Recovery = 30% Analysis Date = 08/05/14 Pct Recovery = 30% Analysis Date = 07/31/14 Pct Recovery = 30% Analysis Date = 07/31/14 Pct Recovery = 30% Analysis Date = 07/26/14 Pct Recovery = 30% Analysis Date = 07/26/14 Pct Recovery = 30% Analysis Date = 07/22/14 Pct Recovery = 30% Analysis Date = 07/22/14 Pct Recovery = 30% Analysis Date = 07/17/14 Pct Recovery = 29% Analysis Date = 07/17/14 Pct Recovery = 29% Analysis Date = 07/13/14 Pct Recovery = 29% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
LOPERAMIDE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 12 53% 15% 45% 19%
>= Reporting Level 28 44% 17% 45% 18%
Total 40 47% 17% 45% 17%

Sample Statistics
LOPERAMIDE

Characteristic N % % Basis
Plotted 40 63% Spiked
Estimated Values 40 63% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 2 3% Spiked
Spiked 63 .  
False Negatives 21 33% 21 out of 63
Not Spiked 52 .  
False Positives 0 0% 0 out of 52

BQS OBSP Determination:
LORATADINE
METHOD: 2440 , TESTIDCODE: 67488LCM56
Open Data Set

Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 38% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 43% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 80 µl & ERA 0406-15-08: 80 µl Pct Recovery = 60% Analysis Date = 11/04/15 SpikeMix = Abs 052215: 80 µl & Abs 050115: 80 µl Pct Recovery = 57% Analysis Date = 01/17/16 SpikeMix = ERA 0406-15-09: 80 µl & ERA 0406-15-07A: 80 µl Pct Recovery = 50% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 80 µl & Abs 051315: 80 µl Pct Recovery = 18% Analysis Date = 11/18/16 SpikeMix = ERA 04281604: 80 µl & ERA 04281603: 80 µl Pct Recovery = 36% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & ERA 04281604: 80 µl Pct Recovery = 38% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 31% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 36% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 33% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 38% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 37% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 36% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-04: 15 µl & Abs 041814: 15 µl Pct Recovery = 48% Analysis Date = 12/06/14 SpikeMix = ERA 0318-14-02: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 47% Analysis Date = 10/25/14 SpikeMix = Abs 041614: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 39% Analysis Date = 10/11/14 SpikeMix = ERA 0318-14-02: 60 µl & ERA 0319-14-04: 60 µl Pct Recovery = 44% Analysis Date = 08/28/14 SpikeMix = ERA 0319-14-04: 60 µl & ERA 0319-14-05: 60 µl Pct Recovery = 48% Analysis Date = 05/07/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 60% Analysis Date = 03/11/15 SpikeMix = ERA 0318-14-02: 15 µl & Abs 041714: 15 µl Pct Recovery = 49% Analysis Date = 01/16/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 52% Analysis Date = 12/06/14 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 47% Analysis Date = 08/21/14 SpikeMix = ERA 0318-14-02: 60 µl & Abs 041714: 60 µl Pct Recovery = 53% Analysis Date = 07/12/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 60% Analysis Date = 06/11/14 SpikeMix = Abs 041614: 60 µl & Abs 041714: 60 µl Pct Recovery = 60% Analysis Date = 05/21/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 62% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 54% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 45% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 62% Analysis Date = 02/23/16 SpikeMix = Abs 052215: 40 µl & Abs 050115: 40 µl Pct Recovery = 65% Analysis Date = 07/31/15 SpikeMix = ERA 0406-15-09: 40 µl & Abs 050115: 40 µl Pct Recovery = 71% Analysis Date = 07/30/15 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 61% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-07A: 40 µl & Abs 051315: 40 µl Pct Recovery = 50% Analysis Date = 11/04/15 SpikeMix = ERA 0406-15-07A: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 48% Analysis Date = 09/10/15 SpikeMix = Abs 052215: 40 µl & ERA 0406-15-07A: 40 µl Pct Recovery = 61% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 29% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 35% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 26% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 31% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 49% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 56% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 44% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 43% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 39% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 39% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 23% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 33% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 26% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 37% Analysis Date = 04/30/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 20% Analysis Date = 04/10/15 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 33% Analysis Date = 02/10/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 45% Analysis Date = 12/07/14 SpikeMix = ERA 0318-14-02: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 46% Analysis Date = 10/11/14 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 30% Analysis Date = 11/04/14 SpikeMix = Abs 041714: 8 µl & ERA 0319-14-05: 8 µl Pct Recovery = 20% Analysis Date = 09/12/14 SpikeMix = Abs 041614: 30 µl & ERA 0319-14-04: 30 µl Pct Recovery = 42% Analysis Date = 08/16/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 57% Analysis Date = 07/13/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 37% Analysis Date = 10/10/14 SpikeMix = Abs 041714: 30 µl & Abs 041814: 30 µl Pct Recovery = 43% Analysis Date = 07/20/14 SpikeMix = ERA 0318-14-02: 30 µl & Abs 041714: 30 µl Pct Recovery = 27% Analysis Date = 06/28/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 42% Analysis Date = 05/17/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 52% Analysis Date = 11/25/15 SpikeMix = Abs 050115: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 51% Analysis Date = 11/24/15 SpikeMix = ERA 0406-15-09: 20 µl & Abs 050115: 20 µl Pct Recovery = 57% Analysis Date = 08/27/15 SpikeMix = Abs 052215: 20 µl & Abs 050115: 20 µl Pct Recovery = 50% Analysis Date = 08/11/15 SpikeMix = Abs 050115: 20 µl & Abs 051315: 20 µl Pct Recovery = 41% Analysis Date = 07/09/15 SpikeMix = Abs 050115: 20 µl & Abs 052215: 20 µl Pct Recovery = 55% Analysis Date = 06/09/15 SpikeMix = Abs 051315: 20 µl & Abs 050115: 20 µl Pct Recovery = 31% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 35% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 33% Analysis Date = 04/27/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 72% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 54% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 49% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 45% Analysis Date = 11/24/15 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 47% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-09: 20 µl Pct Recovery = 2% Analysis Date = 09/15/15 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 59% Analysis Date = 01/18/17 Pct Recovery = 35% Analysis Date = 01/14/17 Pct Recovery = 35% Analysis Date = 01/14/17 Pct Recovery = 35% Analysis Date = 01/09/17 Pct Recovery = 35% Analysis Date = 01/09/17 Pct Recovery = 35% Analysis Date = 01/04/17 Pct Recovery = 35% Analysis Date = 01/04/17 Pct Recovery = 35% Analysis Date = 12/30/16 Pct Recovery = 35% Analysis Date = 12/30/16 Pct Recovery = 35% Analysis Date = 12/25/16 Pct Recovery = 36% Analysis Date = 12/25/16 Pct Recovery = 36% Analysis Date = 12/20/16 Pct Recovery = 36% Analysis Date = 12/20/16 Pct Recovery = 36% Analysis Date = 12/15/16 Pct Recovery = 36% Analysis Date = 12/15/16 Pct Recovery = 36% Analysis Date = 12/10/16 Pct Recovery = 36% Analysis Date = 12/10/16 Pct Recovery = 36% Analysis Date = 12/05/16 Pct Recovery = 36% Analysis Date = 12/05/16 Pct Recovery = 36% Analysis Date = 12/01/16 Pct Recovery = 36% Analysis Date = 12/01/16 Pct Recovery = 36% Analysis Date = 11/26/16 Pct Recovery = 37% Analysis Date = 11/26/16 Pct Recovery = 37% Analysis Date = 11/21/16 Pct Recovery = 37% Analysis Date = 11/21/16 Pct Recovery = 37% Analysis Date = 11/16/16 Pct Recovery = 37% Analysis Date = 11/16/16 Pct Recovery = 37% Analysis Date = 11/11/16 Pct Recovery = 37% Analysis Date = 11/11/16 Pct Recovery = 37% Analysis Date = 11/06/16 Pct Recovery = 37% Analysis Date = 11/06/16 Pct Recovery = 37% Analysis Date = 11/01/16 Pct Recovery = 37% Analysis Date = 11/01/16 Pct Recovery = 37% Analysis Date = 10/27/16 Pct Recovery = 38% Analysis Date = 10/27/16 Pct Recovery = 38% Analysis Date = 10/22/16 Pct Recovery = 38% Analysis Date = 10/22/16 Pct Recovery = 38% Analysis Date = 10/18/16 Pct Recovery = 38% Analysis Date = 10/18/16 Pct Recovery = 38% Analysis Date = 10/13/16 Pct Recovery = 38% Analysis Date = 10/13/16 Pct Recovery = 38% Analysis Date = 10/08/16 Pct Recovery = 38% Analysis Date = 10/08/16 Pct Recovery = 38% Analysis Date = 10/03/16 Pct Recovery = 38% Analysis Date = 10/03/16 Pct Recovery = 38% Analysis Date = 09/28/16 Pct Recovery = 39% Analysis Date = 09/28/16 Pct Recovery = 39% Analysis Date = 09/23/16 Pct Recovery = 39% Analysis Date = 09/23/16 Pct Recovery = 39% Analysis Date = 09/18/16 Pct Recovery = 39% Analysis Date = 09/18/16 Pct Recovery = 39% Analysis Date = 09/13/16 Pct Recovery = 39% Analysis Date = 09/13/16 Pct Recovery = 39% Analysis Date = 09/08/16 Pct Recovery = 39% Analysis Date = 09/08/16 Pct Recovery = 39% Analysis Date = 09/04/16 Pct Recovery = 40% Analysis Date = 09/04/16 Pct Recovery = 40% Analysis Date = 08/30/16 Pct Recovery = 40% Analysis Date = 08/30/16 Pct Recovery = 40% Analysis Date = 08/25/16 Pct Recovery = 40% Analysis Date = 08/25/16 Pct Recovery = 40% Analysis Date = 08/20/16 Pct Recovery = 40% Analysis Date = 08/20/16 Pct Recovery = 40% Analysis Date = 08/15/16 Pct Recovery = 41% Analysis Date = 08/15/16 Pct Recovery = 41% Analysis Date = 08/10/16 Pct Recovery = 41% Analysis Date = 08/10/16 Pct Recovery = 41% Analysis Date = 08/05/16 Pct Recovery = 41% Analysis Date = 08/05/16 Pct Recovery = 41% Analysis Date = 07/31/16 Pct Recovery = 41% Analysis Date = 07/31/16 Pct Recovery = 41% Analysis Date = 07/26/16 Pct Recovery = 41% Analysis Date = 07/26/16 Pct Recovery = 41% Analysis Date = 07/22/16 Pct Recovery = 42% Analysis Date = 07/22/16 Pct Recovery = 42% Analysis Date = 07/17/16 Pct Recovery = 42% Analysis Date = 07/17/16 Pct Recovery = 42% Analysis Date = 07/12/16 Pct Recovery = 42% Analysis Date = 07/12/16 Pct Recovery = 42% Analysis Date = 07/07/16 Pct Recovery = 42% Analysis Date = 07/07/16 Pct Recovery = 42% Analysis Date = 07/02/16 Pct Recovery = 43% Analysis Date = 07/02/16 Pct Recovery = 43% Analysis Date = 06/27/16 Pct Recovery = 43% Analysis Date = 06/27/16 Pct Recovery = 43% Analysis Date = 06/22/16 Pct Recovery = 43% Analysis Date = 06/22/16 Pct Recovery = 43% Analysis Date = 06/17/16 Pct Recovery = 43% Analysis Date = 06/17/16 Pct Recovery = 43% Analysis Date = 06/12/16 Pct Recovery = 44% Analysis Date = 06/12/16 Pct Recovery = 44% Analysis Date = 06/08/16 Pct Recovery = 44% Analysis Date = 06/08/16 Pct Recovery = 44% Analysis Date = 06/03/16 Pct Recovery = 44% Analysis Date = 06/03/16 Pct Recovery = 44% Analysis Date = 05/29/16 Pct Recovery = 44% Analysis Date = 05/29/16 Pct Recovery = 44% Analysis Date = 05/24/16 Pct Recovery = 45% Analysis Date = 05/24/16 Pct Recovery = 45% Analysis Date = 05/19/16 Pct Recovery = 45% Analysis Date = 05/19/16 Pct Recovery = 45% Analysis Date = 05/14/16 Pct Recovery = 45% Analysis Date = 05/14/16 Pct Recovery = 45% Analysis Date = 05/09/16 Pct Recovery = 45% Analysis Date = 05/09/16 Pct Recovery = 45% Analysis Date = 05/04/16 Pct Recovery = 45% Analysis Date = 05/04/16 Pct Recovery = 45% Analysis Date = 04/29/16 Pct Recovery = 46% Analysis Date = 04/29/16 Pct Recovery = 46% Analysis Date = 04/25/16 Pct Recovery = 46% Analysis Date = 04/25/16 Pct Recovery = 46% Analysis Date = 04/20/16 Pct Recovery = 46% Analysis Date = 04/20/16 Pct Recovery = 46% Analysis Date = 04/15/16 Pct Recovery = 46% Analysis Date = 04/15/16 Pct Recovery = 46% Analysis Date = 04/10/16 Pct Recovery = 46% Analysis Date = 04/10/16 Pct Recovery = 46% Analysis Date = 04/05/16 Pct Recovery = 46% Analysis Date = 04/05/16 Pct Recovery = 46% Analysis Date = 03/31/16 Pct Recovery = 46% Analysis Date = 03/31/16 Pct Recovery = 46% Analysis Date = 03/26/16 Pct Recovery = 47% Analysis Date = 03/26/16 Pct Recovery = 47% Analysis Date = 03/21/16 Pct Recovery = 47% Analysis Date = 03/21/16 Pct Recovery = 47% Analysis Date = 03/16/16 Pct Recovery = 47% Analysis Date = 03/16/16 Pct Recovery = 47% Analysis Date = 03/12/16 Pct Recovery = 47% Analysis Date = 03/12/16 Pct Recovery = 47% Analysis Date = 03/07/16 Pct Recovery = 47% Analysis Date = 03/07/16 Pct Recovery = 47% Analysis Date = 03/02/16 Pct Recovery = 47% Analysis Date = 03/02/16 Pct Recovery = 47% Analysis Date = 02/26/16 Pct Recovery = 47% Analysis Date = 02/26/16 Pct Recovery = 47% Analysis Date = 02/21/16 Pct Recovery = 47% Analysis Date = 02/21/16 Pct Recovery = 47% Analysis Date = 02/16/16 Pct Recovery = 47% Analysis Date = 02/16/16 Pct Recovery = 47% Analysis Date = 02/11/16 Pct Recovery = 48% Analysis Date = 02/11/16 Pct Recovery = 48% Analysis Date = 02/06/16 Pct Recovery = 48% Analysis Date = 02/06/16 Pct Recovery = 48% Analysis Date = 02/01/16 Pct Recovery = 48% Analysis Date = 02/01/16 Pct Recovery = 48% Analysis Date = 01/28/16 Pct Recovery = 48% Analysis Date = 01/28/16 Pct Recovery = 48% Analysis Date = 01/23/16 Pct Recovery = 48% Analysis Date = 01/23/16 Pct Recovery = 48% Analysis Date = 01/18/16 Pct Recovery = 48% Analysis Date = 01/18/16 Pct Recovery = 48% Analysis Date = 01/13/16 Pct Recovery = 48% Analysis Date = 01/13/16 Pct Recovery = 48% Analysis Date = 01/08/16 Pct Recovery = 48% Analysis Date = 01/08/16 Pct Recovery = 48% Analysis Date = 01/03/16 Pct Recovery = 48% Analysis Date = 01/03/16 Pct Recovery = 48% Analysis Date = 12/29/15 Pct Recovery = 48% Analysis Date = 12/29/15 Pct Recovery = 48% Analysis Date = 12/24/15 Pct Recovery = 48% Analysis Date = 12/24/15 Pct Recovery = 48% Analysis Date = 12/19/15 Pct Recovery = 48% Analysis Date = 12/19/15 Pct Recovery = 48% Analysis Date = 12/15/15 Pct Recovery = 48% Analysis Date = 12/15/15 Pct Recovery = 48% Analysis Date = 12/10/15 Pct Recovery = 49% Analysis Date = 12/10/15 Pct Recovery = 49% Analysis Date = 12/05/15 Pct Recovery = 49% Analysis Date = 12/05/15 Pct Recovery = 49% Analysis Date = 11/30/15 Pct Recovery = 49% Analysis Date = 11/30/15 Pct Recovery = 49% Analysis Date = 11/25/15 Pct Recovery = 49% Analysis Date = 11/25/15 Pct Recovery = 49% Analysis Date = 11/20/15 Pct Recovery = 49% Analysis Date = 11/20/15 Pct Recovery = 49% Analysis Date = 11/15/15 Pct Recovery = 49% Analysis Date = 11/15/15 Pct Recovery = 49% Analysis Date = 11/10/15 Pct Recovery = 49% Analysis Date = 11/10/15 Pct Recovery = 49% Analysis Date = 11/05/15 Pct Recovery = 48% Analysis Date = 11/05/15 Pct Recovery = 48% Analysis Date = 11/01/15 Pct Recovery = 48% Analysis Date = 11/01/15 Pct Recovery = 48% Analysis Date = 10/27/15 Pct Recovery = 48% Analysis Date = 10/27/15 Pct Recovery = 48% Analysis Date = 10/22/15 Pct Recovery = 48% Analysis Date = 10/22/15 Pct Recovery = 48% Analysis Date = 10/17/15 Pct Recovery = 48% Analysis Date = 10/17/15 Pct Recovery = 48% Analysis Date = 10/12/15 Pct Recovery = 48% Analysis Date = 10/12/15 Pct Recovery = 48% Analysis Date = 10/07/15 Pct Recovery = 48% Analysis Date = 10/07/15 Pct Recovery = 48% Analysis Date = 10/02/15 Pct Recovery = 48% Analysis Date = 10/02/15 Pct Recovery = 48% Analysis Date = 09/27/15 Pct Recovery = 48% Analysis Date = 09/27/15 Pct Recovery = 48% Analysis Date = 09/22/15 Pct Recovery = 48% Analysis Date = 09/22/15 Pct Recovery = 48% Analysis Date = 09/17/15 Pct Recovery = 48% Analysis Date = 09/17/15 Pct Recovery = 48% Analysis Date = 09/13/15 Pct Recovery = 48% Analysis Date = 09/13/15 Pct Recovery = 48% Analysis Date = 09/08/15 Pct Recovery = 47% Analysis Date = 09/08/15 Pct Recovery = 47% Analysis Date = 09/03/15 Pct Recovery = 47% Analysis Date = 09/03/15 Pct Recovery = 47% Analysis Date = 08/29/15 Pct Recovery = 47% Analysis Date = 08/29/15 Pct Recovery = 47% Analysis Date = 08/24/15 Pct Recovery = 47% Analysis Date = 08/24/15 Pct Recovery = 47% Analysis Date = 08/19/15 Pct Recovery = 47% Analysis Date = 08/19/15 Pct Recovery = 47% Analysis Date = 08/14/15 Pct Recovery = 47% Analysis Date = 08/14/15 Pct Recovery = 47% Analysis Date = 08/09/15 Pct Recovery = 47% Analysis Date = 08/09/15 Pct Recovery = 47% Analysis Date = 08/04/15 Pct Recovery = 47% Analysis Date = 08/04/15 Pct Recovery = 47% Analysis Date = 07/31/15 Pct Recovery = 47% Analysis Date = 07/31/15 Pct Recovery = 47% Analysis Date = 07/26/15 Pct Recovery = 47% Analysis Date = 07/26/15 Pct Recovery = 47% Analysis Date = 07/21/15 Pct Recovery = 47% Analysis Date = 07/21/15 Pct Recovery = 47% Analysis Date = 07/16/15 Pct Recovery = 46% Analysis Date = 07/16/15 Pct Recovery = 46% Analysis Date = 07/11/15 Pct Recovery = 46% Analysis Date = 07/11/15 Pct Recovery = 46% Analysis Date = 07/06/15 Pct Recovery = 46% Analysis Date = 07/06/15 Pct Recovery = 46% Analysis Date = 07/01/15 Pct Recovery = 46% Analysis Date = 07/01/15 Pct Recovery = 46% Analysis Date = 06/26/15 Pct Recovery = 46% Analysis Date = 06/26/15 Pct Recovery = 46% Analysis Date = 06/21/15 Pct Recovery = 46% Analysis Date = 06/21/15 Pct Recovery = 46% Analysis Date = 06/17/15 Pct Recovery = 46% Analysis Date = 06/17/15 Pct Recovery = 46% Analysis Date = 06/12/15 Pct Recovery = 46% Analysis Date = 06/12/15 Pct Recovery = 46% Analysis Date = 06/07/15 Pct Recovery = 46% Analysis Date = 06/07/15 Pct Recovery = 46% Analysis Date = 06/02/15 Pct Recovery = 46% Analysis Date = 06/02/15 Pct Recovery = 46% Analysis Date = 05/28/15 Pct Recovery = 45% Analysis Date = 05/28/15 Pct Recovery = 45% Analysis Date = 05/23/15 Pct Recovery = 45% Analysis Date = 05/23/15 Pct Recovery = 45% Analysis Date = 05/18/15 Pct Recovery = 45% Analysis Date = 05/18/15 Pct Recovery = 45% Analysis Date = 05/13/15 Pct Recovery = 45% Analysis Date = 05/13/15 Pct Recovery = 45% Analysis Date = 05/08/15 Pct Recovery = 45% Analysis Date = 05/08/15 Pct Recovery = 45% Analysis Date = 05/04/15 Pct Recovery = 45% Analysis Date = 05/04/15 Pct Recovery = 45% Analysis Date = 04/29/15 Pct Recovery = 45% Analysis Date = 04/29/15 Pct Recovery = 45% Analysis Date = 04/24/15 Pct Recovery = 45% Analysis Date = 04/24/15 Pct Recovery = 45% Analysis Date = 04/19/15 Pct Recovery = 45% Analysis Date = 04/19/15 Pct Recovery = 45% Analysis Date = 04/14/15 Pct Recovery = 45% Analysis Date = 04/14/15 Pct Recovery = 45% Analysis Date = 04/09/15 Pct Recovery = 45% Analysis Date = 04/09/15 Pct Recovery = 45% Analysis Date = 04/04/15 Pct Recovery = 45% Analysis Date = 04/04/15 Pct Recovery = 45% Analysis Date = 03/30/15 Pct Recovery = 45% Analysis Date = 03/30/15 Pct Recovery = 45% Analysis Date = 03/25/15 Pct Recovery = 45% Analysis Date = 03/25/15 Pct Recovery = 45% Analysis Date = 03/21/15 Pct Recovery = 45% Analysis Date = 03/21/15 Pct Recovery = 45% Analysis Date = 03/16/15 Pct Recovery = 45% Analysis Date = 03/16/15 Pct Recovery = 45% Analysis Date = 03/11/15 Pct Recovery = 45% Analysis Date = 03/11/15 Pct Recovery = 45% Analysis Date = 03/06/15 Pct Recovery = 45% Analysis Date = 03/06/15 Pct Recovery = 45% Analysis Date = 03/01/15 Pct Recovery = 45% Analysis Date = 03/01/15 Pct Recovery = 45% Analysis Date = 02/24/15 Pct Recovery = 45% Analysis Date = 02/24/15 Pct Recovery = 45% Analysis Date = 02/19/15 Pct Recovery = 45% Analysis Date = 02/19/15 Pct Recovery = 45% Analysis Date = 02/14/15 Pct Recovery = 45% Analysis Date = 02/14/15 Pct Recovery = 45% Analysis Date = 02/09/15 Pct Recovery = 45% Analysis Date = 02/09/15 Pct Recovery = 45% Analysis Date = 02/05/15 Pct Recovery = 45% Analysis Date = 02/05/15 Pct Recovery = 45% Analysis Date = 01/31/15 Pct Recovery = 45% Analysis Date = 01/31/15 Pct Recovery = 45% Analysis Date = 01/26/15 Pct Recovery = 45% Analysis Date = 01/26/15 Pct Recovery = 45% Analysis Date = 01/21/15 Pct Recovery = 45% Analysis Date = 01/21/15 Pct Recovery = 45% Analysis Date = 01/16/15 Pct Recovery = 45% Analysis Date = 01/16/15 Pct Recovery = 45% Analysis Date = 01/11/15 Pct Recovery = 45% Analysis Date = 01/11/15 Pct Recovery = 45% Analysis Date = 01/06/15 Pct Recovery = 45% Analysis Date = 01/06/15 Pct Recovery = 45% Analysis Date = 01/01/15 Pct Recovery = 45% Analysis Date = 01/01/15 Pct Recovery = 45% Analysis Date = 12/27/14 Pct Recovery = 45% Analysis Date = 12/27/14 Pct Recovery = 45% Analysis Date = 12/23/14 Pct Recovery = 45% Analysis Date = 12/23/14 Pct Recovery = 45% Analysis Date = 12/18/14 Pct Recovery = 45% Analysis Date = 12/18/14 Pct Recovery = 45% Analysis Date = 12/13/14 Pct Recovery = 45% Analysis Date = 12/13/14 Pct Recovery = 45% Analysis Date = 12/08/14 Pct Recovery = 45% Analysis Date = 12/08/14 Pct Recovery = 45% Analysis Date = 12/03/14 Pct Recovery = 45% Analysis Date = 12/03/14 Pct Recovery = 45% Analysis Date = 11/28/14 Pct Recovery = 45% Analysis Date = 11/28/14 Pct Recovery = 45% Analysis Date = 11/23/14 Pct Recovery = 45% Analysis Date = 11/23/14 Pct Recovery = 45% Analysis Date = 11/18/14 Pct Recovery = 45% Analysis Date = 11/18/14 Pct Recovery = 45% Analysis Date = 11/13/14 Pct Recovery = 45% Analysis Date = 11/13/14 Pct Recovery = 45% Analysis Date = 11/09/14 Pct Recovery = 45% Analysis Date = 11/09/14 Pct Recovery = 45% Analysis Date = 11/04/14 Pct Recovery = 45% Analysis Date = 11/04/14 Pct Recovery = 45% Analysis Date = 10/30/14 Pct Recovery = 45% Analysis Date = 10/30/14 Pct Recovery = 45% Analysis Date = 10/25/14 Pct Recovery = 45% Analysis Date = 10/25/14 Pct Recovery = 45% Analysis Date = 10/20/14 Pct Recovery = 45% Analysis Date = 10/20/14 Pct Recovery = 45% Analysis Date = 10/15/14 Pct Recovery = 45% Analysis Date = 10/15/14 Pct Recovery = 45% Analysis Date = 10/10/14 Pct Recovery = 45% Analysis Date = 10/10/14 Pct Recovery = 45% Analysis Date = 10/05/14 Pct Recovery = 46% Analysis Date = 10/05/14 Pct Recovery = 46% Analysis Date = 09/30/14 Pct Recovery = 46% Analysis Date = 09/30/14 Pct Recovery = 46% Analysis Date = 09/26/14 Pct Recovery = 46% Analysis Date = 09/26/14 Pct Recovery = 46% Analysis Date = 09/21/14 Pct Recovery = 46% Analysis Date = 09/21/14 Pct Recovery = 46% Analysis Date = 09/16/14 Pct Recovery = 46% Analysis Date = 09/16/14 Pct Recovery = 46% Analysis Date = 09/11/14 Pct Recovery = 46% Analysis Date = 09/11/14 Pct Recovery = 46% Analysis Date = 09/06/14 Pct Recovery = 46% Analysis Date = 09/06/14 Pct Recovery = 46% Analysis Date = 09/01/14 Pct Recovery = 46% Analysis Date = 09/01/14 Pct Recovery = 46% Analysis Date = 08/27/14 Pct Recovery = 46% Analysis Date = 08/27/14 Pct Recovery = 46% Analysis Date = 08/22/14 Pct Recovery = 46% Analysis Date = 08/22/14 Pct Recovery = 46% Analysis Date = 08/17/14 Pct Recovery = 46% Analysis Date = 08/17/14 Pct Recovery = 46% Analysis Date = 08/13/14 Pct Recovery = 46% Analysis Date = 08/13/14 Pct Recovery = 46% Analysis Date = 08/08/14 Pct Recovery = 46% Analysis Date = 08/08/14 Pct Recovery = 46% Analysis Date = 08/03/14 Pct Recovery = 46% Analysis Date = 08/03/14 Pct Recovery = 46% Analysis Date = 07/29/14 Pct Recovery = 46% Analysis Date = 07/29/14 Pct Recovery = 46% Analysis Date = 07/24/14 Pct Recovery = 46% Analysis Date = 07/24/14 Pct Recovery = 46% Analysis Date = 07/19/14 Pct Recovery = 46% Analysis Date = 07/19/14 Pct Recovery = 46% Analysis Date = 07/14/14 Pct Recovery = 46% Analysis Date = 07/14/14 Pct Recovery = 46% Analysis Date = 07/09/14 Pct Recovery = 46% Analysis Date = 07/09/14 Pct Recovery = 46% Analysis Date = 07/04/14 Pct Recovery = 46% Analysis Date = 07/04/14 Pct Recovery = 46% Analysis Date = 06/30/14 Pct Recovery = 46% Analysis Date = 06/30/14 Pct Recovery = 46% Analysis Date = 06/25/14 Pct Recovery = 46% Analysis Date = 06/25/14 Pct Recovery = 46% Analysis Date = 06/20/14 Pct Recovery = 46% Analysis Date = 06/20/14 Pct Recovery = 46% Analysis Date = 06/15/14 Pct Recovery = 47% Analysis Date = 06/15/14 Pct Recovery = 47% Analysis Date = 06/10/14 Pct Recovery = 47% Analysis Date = 06/10/14 Pct Recovery = 47% Analysis Date = 06/05/14 Pct Recovery = 47% Analysis Date = 06/05/14 Pct Recovery = 47% Analysis Date = 05/31/14 Pct Recovery = 47% Analysis Date = 05/31/14 Pct Recovery = 47% Analysis Date = 05/26/14 Pct Recovery = 47% Analysis Date = 05/26/14 Pct Recovery = 47% Analysis Date = 05/21/14 Pct Recovery = 47% Analysis Date = 05/21/14 Pct Recovery = 47% Analysis Date = 05/17/14 Pct Recovery = 47% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
LORATADINE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 78 44% 13% 44% 12%
Total 78 44% 13% 44% 12%

Sample Statistics
LORATADINE

Characteristic N % % Basis
Plotted 78 100% Spiked
Estimated Values 38 49% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 78 .  
False Negatives 0 0% 0 out of 78
Not Spiked 37 .  
False Positives 0 0% 0 out of 37

BQS OBSP Determination:
LORAZEPAM
METHOD: 2440 , TESTIDCODE: 67470LCM56
Open Data Set

Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 148% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 129% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 80 µl & ERA 0406-15-08: 80 µl Pct Recovery = 99% Analysis Date = 11/04/15 SpikeMix = Abs 052215: 80 µl & Abs 050115: 80 µl Pct Recovery = 102% Analysis Date = 11/18/16 SpikeMix = ERA 04281604: 80 µl & ERA 04281603: 80 µl Pct Recovery = 98% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & ERA 04281604: 80 µl Pct Recovery = 111% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 92% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 93% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 104% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 98% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 124% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 122% Analysis Date = 05/07/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 125% Analysis Date = 03/11/15 SpikeMix = ERA 0318-14-02: 15 µl & Abs 041714: 15 µl Pct Recovery = 114% Analysis Date = 01/16/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 108% Analysis Date = 12/06/14 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 95% Analysis Date = 08/21/14 SpikeMix = ERA 0318-14-02: 60 µl & Abs 041714: 60 µl Pct Recovery = 89% Analysis Date = 07/12/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 78% Analysis Date = 06/11/14 SpikeMix = Abs 041614: 60 µl & Abs 041714: 60 µl Pct Recovery = 105% Analysis Date = 05/21/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 94% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 111% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 93% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 72% Analysis Date = 02/23/16 SpikeMix = Abs 052215: 40 µl & Abs 050115: 40 µl Pct Recovery = 45% Analysis Date = 07/30/15 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 105% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 117% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 103% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 71% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 83% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 128% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 195% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 153% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 118% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 99% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 109% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 110% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 101% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 116% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 155% Analysis Date = 11/04/14 SpikeMix = Abs 041714: 8 µl & ERA 0319-14-05: 8 µl Pct Recovery = 81% Analysis Date = 10/10/14 SpikeMix = Abs 041714: 30 µl & Abs 041814: 30 µl Pct Recovery = 68% Analysis Date = 07/20/14 SpikeMix = ERA 0318-14-02: 30 µl & Abs 041714: 30 µl Pct Recovery = 86% Analysis Date = 06/28/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 91% Analysis Date = 05/17/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 58% Analysis Date = 11/25/15 SpikeMix = Abs 050115: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 151% Analysis Date = 11/24/15 SpikeMix = ERA 0406-15-09: 20 µl & Abs 050115: 20 µl Pct Recovery = 104% Analysis Date = 08/27/15 SpikeMix = Abs 052215: 20 µl & Abs 050115: 20 µl Pct Recovery = 140% Analysis Date = 07/09/15 SpikeMix = Abs 050115: 20 µl & Abs 052215: 20 µl Pct Recovery = 85% Analysis Date = 06/09/15 SpikeMix = Abs 051315: 20 µl & Abs 050115: 20 µl Pct Recovery = 105% Analysis Date = 01/18/17 Pct Recovery = 132% Analysis Date = 01/14/17 Pct Recovery = 131% Analysis Date = 01/14/17 Pct Recovery = 131% Analysis Date = 01/09/17 Pct Recovery = 130% Analysis Date = 01/09/17 Pct Recovery = 130% Analysis Date = 01/04/17 Pct Recovery = 129% Analysis Date = 01/04/17 Pct Recovery = 129% Analysis Date = 12/30/16 Pct Recovery = 129% Analysis Date = 12/30/16 Pct Recovery = 129% Analysis Date = 12/25/16 Pct Recovery = 128% Analysis Date = 12/25/16 Pct Recovery = 128% Analysis Date = 12/20/16 Pct Recovery = 127% Analysis Date = 12/20/16 Pct Recovery = 127% Analysis Date = 12/15/16 Pct Recovery = 126% Analysis Date = 12/15/16 Pct Recovery = 126% Analysis Date = 12/10/16 Pct Recovery = 125% Analysis Date = 12/10/16 Pct Recovery = 125% Analysis Date = 12/05/16 Pct Recovery = 124% Analysis Date = 12/05/16 Pct Recovery = 124% Analysis Date = 12/01/16 Pct Recovery = 123% Analysis Date = 12/01/16 Pct Recovery = 123% Analysis Date = 11/26/16 Pct Recovery = 122% Analysis Date = 11/26/16 Pct Recovery = 122% Analysis Date = 11/21/16 Pct Recovery = 121% Analysis Date = 11/21/16 Pct Recovery = 121% Analysis Date = 11/16/16 Pct Recovery = 121% Analysis Date = 11/16/16 Pct Recovery = 121% Analysis Date = 11/11/16 Pct Recovery = 120% Analysis Date = 11/11/16 Pct Recovery = 120% Analysis Date = 11/06/16 Pct Recovery = 119% Analysis Date = 11/06/16 Pct Recovery = 119% Analysis Date = 11/01/16 Pct Recovery = 118% Analysis Date = 11/01/16 Pct Recovery = 118% Analysis Date = 10/27/16 Pct Recovery = 117% Analysis Date = 10/27/16 Pct Recovery = 117% Analysis Date = 10/22/16 Pct Recovery = 117% Analysis Date = 10/22/16 Pct Recovery = 117% Analysis Date = 10/18/16 Pct Recovery = 116% Analysis Date = 10/18/16 Pct Recovery = 116% Analysis Date = 10/13/16 Pct Recovery = 115% Analysis Date = 10/13/16 Pct Recovery = 115% Analysis Date = 10/08/16 Pct Recovery = 114% Analysis Date = 10/08/16 Pct Recovery = 114% Analysis Date = 10/03/16 Pct Recovery = 114% Analysis Date = 10/03/16 Pct Recovery = 114% Analysis Date = 09/28/16 Pct Recovery = 113% Analysis Date = 09/28/16 Pct Recovery = 113% Analysis Date = 09/23/16 Pct Recovery = 112% Analysis Date = 09/23/16 Pct Recovery = 112% Analysis Date = 09/18/16 Pct Recovery = 112% Analysis Date = 09/18/16 Pct Recovery = 112% Analysis Date = 09/13/16 Pct Recovery = 111% Analysis Date = 09/13/16 Pct Recovery = 111% Analysis Date = 09/08/16 Pct Recovery = 111% Analysis Date = 09/08/16 Pct Recovery = 111% Analysis Date = 09/04/16 Pct Recovery = 111% Analysis Date = 09/04/16 Pct Recovery = 111% Analysis Date = 08/30/16 Pct Recovery = 111% Analysis Date = 08/30/16 Pct Recovery = 111% Analysis Date = 08/25/16 Pct Recovery = 110% Analysis Date = 08/25/16 Pct Recovery = 110% Analysis Date = 08/20/16 Pct Recovery = 110% Analysis Date = 08/20/16 Pct Recovery = 110% Analysis Date = 08/15/16 Pct Recovery = 110% Analysis Date = 08/15/16 Pct Recovery = 110% Analysis Date = 08/10/16 Pct Recovery = 110% Analysis Date = 08/10/16 Pct Recovery = 110% Analysis Date = 08/05/16 Pct Recovery = 110% Analysis Date = 08/05/16 Pct Recovery = 110% Analysis Date = 07/31/16 Pct Recovery = 109% Analysis Date = 07/31/16 Pct Recovery = 109% Analysis Date = 07/26/16 Pct Recovery = 109% Analysis Date = 07/26/16 Pct Recovery = 109% Analysis Date = 07/22/16 Pct Recovery = 108% Analysis Date = 07/22/16 Pct Recovery = 108% Analysis Date = 07/17/16 Pct Recovery = 108% Analysis Date = 07/17/16 Pct Recovery = 108% Analysis Date = 07/12/16 Pct Recovery = 107% Analysis Date = 07/12/16 Pct Recovery = 107% Analysis Date = 07/07/16 Pct Recovery = 107% Analysis Date = 07/07/16 Pct Recovery = 107% Analysis Date = 07/02/16 Pct Recovery = 107% Analysis Date = 07/02/16 Pct Recovery = 107% Analysis Date = 06/27/16 Pct Recovery = 106% Analysis Date = 06/27/16 Pct Recovery = 106% Analysis Date = 06/22/16 Pct Recovery = 106% Analysis Date = 06/22/16 Pct Recovery = 106% Analysis Date = 06/17/16 Pct Recovery = 105% Analysis Date = 06/17/16 Pct Recovery = 105% Analysis Date = 06/12/16 Pct Recovery = 105% Analysis Date = 06/12/16 Pct Recovery = 105% Analysis Date = 06/08/16 Pct Recovery = 104% Analysis Date = 06/08/16 Pct Recovery = 104% Analysis Date = 06/03/16 Pct Recovery = 104% Analysis Date = 06/03/16 Pct Recovery = 104% Analysis Date = 05/29/16 Pct Recovery = 103% Analysis Date = 05/29/16 Pct Recovery = 103% Analysis Date = 05/24/16 Pct Recovery = 103% Analysis Date = 05/24/16 Pct Recovery = 103% Analysis Date = 05/19/16 Pct Recovery = 102% Analysis Date = 05/19/16 Pct Recovery = 102% Analysis Date = 05/14/16 Pct Recovery = 102% Analysis Date = 05/14/16 Pct Recovery = 102% Analysis Date = 05/09/16 Pct Recovery = 101% Analysis Date = 05/09/16 Pct Recovery = 101% Analysis Date = 05/04/16 Pct Recovery = 101% Analysis Date = 05/04/16 Pct Recovery = 101% Analysis Date = 04/29/16 Pct Recovery = 100% Analysis Date = 04/29/16 Pct Recovery = 100% Analysis Date = 04/25/16 Pct Recovery = 100% Analysis Date = 04/25/16 Pct Recovery = 100% Analysis Date = 04/20/16 Pct Recovery = 100% Analysis Date = 04/20/16 Pct Recovery = 100% Analysis Date = 04/15/16 Pct Recovery = 101% Analysis Date = 04/15/16 Pct Recovery = 101% Analysis Date = 04/10/16 Pct Recovery = 101% Analysis Date = 04/10/16 Pct Recovery = 101% Analysis Date = 04/05/16 Pct Recovery = 101% Analysis Date = 04/05/16 Pct Recovery = 101% Analysis Date = 03/31/16 Pct Recovery = 101% Analysis Date = 03/31/16 Pct Recovery = 101% Analysis Date = 03/26/16 Pct Recovery = 102% Analysis Date = 03/26/16 Pct Recovery = 102% Analysis Date = 03/21/16 Pct Recovery = 102% Analysis Date = 03/21/16 Pct Recovery = 102% Analysis Date = 03/16/16 Pct Recovery = 102% Analysis Date = 03/16/16 Pct Recovery = 102% Analysis Date = 03/12/16 Pct Recovery = 102% Analysis Date = 03/12/16 Pct Recovery = 102% Analysis Date = 03/07/16 Pct Recovery = 103% Analysis Date = 03/07/16 Pct Recovery = 103% Analysis Date = 03/02/16 Pct Recovery = 103% Analysis Date = 03/02/16 Pct Recovery = 103% Analysis Date = 02/26/16 Pct Recovery = 103% Analysis Date = 02/26/16 Pct Recovery = 103% Analysis Date = 02/21/16 Pct Recovery = 103% Analysis Date = 02/21/16 Pct Recovery = 103% Analysis Date = 02/16/16 Pct Recovery = 103% Analysis Date = 02/16/16 Pct Recovery = 103% Analysis Date = 02/11/16 Pct Recovery = 103% Analysis Date = 02/11/16 Pct Recovery = 103% Analysis Date = 02/06/16 Pct Recovery = 104% Analysis Date = 02/06/16 Pct Recovery = 104% Analysis Date = 02/01/16 Pct Recovery = 104% Analysis Date = 02/01/16 Pct Recovery = 104% Analysis Date = 01/28/16 Pct Recovery = 104% Analysis Date = 01/28/16 Pct Recovery = 104% Analysis Date = 01/23/16 Pct Recovery = 104% Analysis Date = 01/23/16 Pct Recovery = 104% Analysis Date = 01/18/16 Pct Recovery = 104% Analysis Date = 01/18/16 Pct Recovery = 104% Analysis Date = 01/13/16 Pct Recovery = 104% Analysis Date = 01/13/16 Pct Recovery = 104% Analysis Date = 01/08/16 Pct Recovery = 104% Analysis Date = 01/08/16 Pct Recovery = 104% Analysis Date = 01/03/16 Pct Recovery = 104% Analysis Date = 01/03/16 Pct Recovery = 104% Analysis Date = 12/29/15 Pct Recovery = 104% Analysis Date = 12/29/15 Pct Recovery = 104% Analysis Date = 12/24/15 Pct Recovery = 104% Analysis Date = 12/24/15 Pct Recovery = 104% Analysis Date = 12/19/15 Pct Recovery = 104% Analysis Date = 12/19/15 Pct Recovery = 104% Analysis Date = 12/15/15 Pct Recovery = 105% Analysis Date = 12/15/15 Pct Recovery = 105% Analysis Date = 12/10/15 Pct Recovery = 105% Analysis Date = 12/10/15 Pct Recovery = 105% Analysis Date = 12/05/15 Pct Recovery = 105% Analysis Date = 12/05/15 Pct Recovery = 105% Analysis Date = 11/30/15 Pct Recovery = 105% Analysis Date = 11/30/15 Pct Recovery = 105% Analysis Date = 11/25/15 Pct Recovery = 105% Analysis Date = 11/25/15 Pct Recovery = 105% Analysis Date = 11/20/15 Pct Recovery = 105% Analysis Date = 11/20/15 Pct Recovery = 105% Analysis Date = 11/15/15 Pct Recovery = 105% Analysis Date = 11/15/15 Pct Recovery = 105% Analysis Date = 11/10/15 Pct Recovery = 105% Analysis Date = 11/10/15 Pct Recovery = 105% Analysis Date = 11/05/15 Pct Recovery = 105% Analysis Date = 11/05/15 Pct Recovery = 105% Analysis Date = 11/01/15 Pct Recovery = 105% Analysis Date = 11/01/15 Pct Recovery = 105% Analysis Date = 10/27/15 Pct Recovery = 105% Analysis Date = 10/27/15 Pct Recovery = 105% Analysis Date = 10/22/15 Pct Recovery = 105% Analysis Date = 10/22/15 Pct Recovery = 105% Analysis Date = 10/17/15 Pct Recovery = 105% Analysis Date = 10/17/15 Pct Recovery = 105% Analysis Date = 10/12/15 Pct Recovery = 105% Analysis Date = 10/12/15 Pct Recovery = 105% Analysis Date = 10/07/15 Pct Recovery = 105% Analysis Date = 10/07/15 Pct Recovery = 105% Analysis Date = 10/02/15 Pct Recovery = 105% Analysis Date = 10/02/15 Pct Recovery = 105% Analysis Date = 09/27/15 Pct Recovery = 105% Analysis Date = 09/27/15 Pct Recovery = 105% Analysis Date = 09/22/15 Pct Recovery = 105% Analysis Date = 09/22/15 Pct Recovery = 105% Analysis Date = 09/17/15 Pct Recovery = 105% Analysis Date = 09/17/15 Pct Recovery = 105% Analysis Date = 09/13/15 Pct Recovery = 105% Analysis Date = 09/13/15 Pct Recovery = 105% Analysis Date = 09/08/15 Pct Recovery = 105% Analysis Date = 09/08/15 Pct Recovery = 105% Analysis Date = 09/03/15 Pct Recovery = 105% Analysis Date = 09/03/15 Pct Recovery = 105% Analysis Date = 08/29/15 Pct Recovery = 105% Analysis Date = 08/29/15 Pct Recovery = 105% Analysis Date = 08/24/15 Pct Recovery = 105% Analysis Date = 08/24/15 Pct Recovery = 105% Analysis Date = 08/19/15 Pct Recovery = 105% Analysis Date = 08/19/15 Pct Recovery = 105% Analysis Date = 08/14/15 Pct Recovery = 105% Analysis Date = 08/14/15 Pct Recovery = 105% Analysis Date = 08/09/15 Pct Recovery = 105% Analysis Date = 08/09/15 Pct Recovery = 105% Analysis Date = 08/04/15 Pct Recovery = 105% Analysis Date = 08/04/15 Pct Recovery = 105% Analysis Date = 07/31/15 Pct Recovery = 105% Analysis Date = 07/31/15 Pct Recovery = 105% Analysis Date = 07/26/15 Pct Recovery = 105% Analysis Date = 07/26/15 Pct Recovery = 105% Analysis Date = 07/21/15 Pct Recovery = 104% Analysis Date = 07/21/15 Pct Recovery = 104% Analysis Date = 07/16/15 Pct Recovery = 104% Analysis Date = 07/16/15 Pct Recovery = 104% Analysis Date = 07/11/15 Pct Recovery = 104% Analysis Date = 07/11/15 Pct Recovery = 104% Analysis Date = 07/06/15 Pct Recovery = 104% Analysis Date = 07/06/15 Pct Recovery = 104% Analysis Date = 07/01/15 Pct Recovery = 104% Analysis Date = 07/01/15 Pct Recovery = 104% Analysis Date = 06/26/15 Pct Recovery = 103% Analysis Date = 06/26/15 Pct Recovery = 103% Analysis Date = 06/21/15 Pct Recovery = 103% Analysis Date = 06/21/15 Pct Recovery = 103% Analysis Date = 06/17/15 Pct Recovery = 103% Analysis Date = 06/17/15 Pct Recovery = 103% Analysis Date = 06/12/15 Pct Recovery = 103% Analysis Date = 06/12/15 Pct Recovery = 103% Analysis Date = 06/07/15 Pct Recovery = 102% Analysis Date = 06/07/15 Pct Recovery = 102% Analysis Date = 06/02/15 Pct Recovery = 102% Analysis Date = 06/02/15 Pct Recovery = 102% Analysis Date = 05/28/15 Pct Recovery = 102% Analysis Date = 05/28/15 Pct Recovery = 102% Analysis Date = 05/23/15 Pct Recovery = 102% Analysis Date = 05/23/15 Pct Recovery = 102% Analysis Date = 05/18/15 Pct Recovery = 102% Analysis Date = 05/18/15 Pct Recovery = 102% Analysis Date = 05/13/15 Pct Recovery = 101% Analysis Date = 05/13/15 Pct Recovery = 101% Analysis Date = 05/08/15 Pct Recovery = 101% Analysis Date = 05/08/15 Pct Recovery = 101% Analysis Date = 05/04/15 Pct Recovery = 101% Analysis Date = 05/04/15 Pct Recovery = 101% Analysis Date = 04/29/15 Pct Recovery = 101% Analysis Date = 04/29/15 Pct Recovery = 101% Analysis Date = 04/24/15 Pct Recovery = 101% Analysis Date = 04/24/15 Pct Recovery = 101% Analysis Date = 04/19/15 Pct Recovery = 100% Analysis Date = 04/19/15 Pct Recovery = 100% Analysis Date = 04/14/15 Pct Recovery = 100% Analysis Date = 04/14/15 Pct Recovery = 100% Analysis Date = 04/09/15 Pct Recovery = 100% Analysis Date = 04/09/15 Pct Recovery = 100% Analysis Date = 04/04/15 Pct Recovery = 100% Analysis Date = 04/04/15 Pct Recovery = 100% Analysis Date = 03/30/15 Pct Recovery = 99% Analysis Date = 03/30/15 Pct Recovery = 99% Analysis Date = 03/25/15 Pct Recovery = 99% Analysis Date = 03/25/15 Pct Recovery = 99% Analysis Date = 03/21/15 Pct Recovery = 99% Analysis Date = 03/21/15 Pct Recovery = 99% Analysis Date = 03/16/15 Pct Recovery = 99% Analysis Date = 03/16/15 Pct Recovery = 99% Analysis Date = 03/11/15 Pct Recovery = 99% Analysis Date = 03/11/15 Pct Recovery = 99% Analysis Date = 03/06/15 Pct Recovery = 98% Analysis Date = 03/06/15 Pct Recovery = 98% Analysis Date = 03/01/15 Pct Recovery = 98% Analysis Date = 03/01/15 Pct Recovery = 98% Analysis Date = 02/24/15 Pct Recovery = 98% Analysis Date = 02/24/15 Pct Recovery = 98% Analysis Date = 02/19/15 Pct Recovery = 98% Analysis Date = 02/19/15 Pct Recovery = 98% Analysis Date = 02/14/15 Pct Recovery = 97% Analysis Date = 02/14/15 Pct Recovery = 97% Analysis Date = 02/09/15 Pct Recovery = 97% Analysis Date = 02/09/15 Pct Recovery = 97% Analysis Date = 02/05/15 Pct Recovery = 97% Analysis Date = 02/05/15 Pct Recovery = 97% Analysis Date = 01/31/15 Pct Recovery = 97% Analysis Date = 01/31/15 Pct Recovery = 97% Analysis Date = 01/26/15 Pct Recovery = 96% Analysis Date = 01/26/15 Pct Recovery = 96% Analysis Date = 01/21/15 Pct Recovery = 96% Analysis Date = 01/21/15 Pct Recovery = 96% Analysis Date = 01/16/15 Pct Recovery = 96% Analysis Date = 01/16/15 Pct Recovery = 96% Analysis Date = 01/11/15 Pct Recovery = 96% Analysis Date = 01/11/15 Pct Recovery = 96% Analysis Date = 01/06/15 Pct Recovery = 96% Analysis Date = 01/06/15 Pct Recovery = 96% Analysis Date = 01/01/15 Pct Recovery = 95% Analysis Date = 01/01/15 Pct Recovery = 95% Analysis Date = 12/27/14 Pct Recovery = 95% Analysis Date = 12/27/14 Pct Recovery = 95% Analysis Date = 12/23/14 Pct Recovery = 95% Analysis Date = 12/23/14 Pct Recovery = 95% Analysis Date = 12/18/14 Pct Recovery = 95% Analysis Date = 12/18/14 Pct Recovery = 95% Analysis Date = 12/13/14 Pct Recovery = 94% Analysis Date = 12/13/14 Pct Recovery = 94% Analysis Date = 12/08/14 Pct Recovery = 94% Analysis Date = 12/08/14 Pct Recovery = 94% Analysis Date = 12/03/14 Pct Recovery = 94% Analysis Date = 12/03/14 Pct Recovery = 94% Analysis Date = 11/28/14 Pct Recovery = 94% Analysis Date = 11/28/14 Pct Recovery = 94% Analysis Date = 11/23/14 Pct Recovery = 93% Analysis Date = 11/23/14 Pct Recovery = 93% Analysis Date = 11/18/14 Pct Recovery = 93% Analysis Date = 11/18/14 Pct Recovery = 93% Analysis Date = 11/13/14 Pct Recovery = 93% Analysis Date = 11/13/14 Pct Recovery = 93% Analysis Date = 11/09/14 Pct Recovery = 93% Analysis Date = 11/09/14 Pct Recovery = 93% Analysis Date = 11/04/14 Pct Recovery = 92% Analysis Date = 11/04/14 Pct Recovery = 92% Analysis Date = 10/30/14 Pct Recovery = 92% Analysis Date = 10/30/14 Pct Recovery = 92% Analysis Date = 10/25/14 Pct Recovery = 92% Analysis Date = 10/25/14 Pct Recovery = 92% Analysis Date = 10/20/14 Pct Recovery = 92% Analysis Date = 10/20/14 Pct Recovery = 92% Analysis Date = 10/15/14 Pct Recovery = 91% Analysis Date = 10/15/14 Pct Recovery = 91% Analysis Date = 10/10/14 Pct Recovery = 91% Analysis Date = 10/10/14 Pct Recovery = 91% Analysis Date = 10/05/14 Pct Recovery = 91% Analysis Date = 10/05/14 Pct Recovery = 91% Analysis Date = 09/30/14 Pct Recovery = 91% Analysis Date = 09/30/14 Pct Recovery = 91% Analysis Date = 09/26/14 Pct Recovery = 90% Analysis Date = 09/26/14 Pct Recovery = 90% Analysis Date = 09/21/14 Pct Recovery = 90% Analysis Date = 09/21/14 Pct Recovery = 90% Analysis Date = 09/16/14 Pct Recovery = 90% Analysis Date = 09/16/14 Pct Recovery = 90% Analysis Date = 09/11/14 Pct Recovery = 90% Analysis Date = 09/11/14 Pct Recovery = 90% Analysis Date = 09/06/14 Pct Recovery = 89% Analysis Date = 09/06/14 Pct Recovery = 89% Analysis Date = 09/01/14 Pct Recovery = 89% Analysis Date = 09/01/14 Pct Recovery = 89% Analysis Date = 08/27/14 Pct Recovery = 89% Analysis Date = 08/27/14 Pct Recovery = 89% Analysis Date = 08/22/14 Pct Recovery = 89% Analysis Date = 08/22/14 Pct Recovery = 89% Analysis Date = 08/17/14 Pct Recovery = 88% Analysis Date = 08/17/14 Pct Recovery = 88% Analysis Date = 08/13/14 Pct Recovery = 88% Analysis Date = 08/13/14 Pct Recovery = 88% Analysis Date = 08/08/14 Pct Recovery = 88% Analysis Date = 08/08/14 Pct Recovery = 88% Analysis Date = 08/03/14 Pct Recovery = 87% Analysis Date = 08/03/14 Pct Recovery = 87% Analysis Date = 07/29/14 Pct Recovery = 87% Analysis Date = 07/29/14 Pct Recovery = 87% Analysis Date = 07/24/14 Pct Recovery = 87% Analysis Date = 07/24/14 Pct Recovery = 87% Analysis Date = 07/19/14 Pct Recovery = 87% Analysis Date = 07/19/14 Pct Recovery = 87% Analysis Date = 07/14/14 Pct Recovery = 86% Analysis Date = 07/14/14 Pct Recovery = 86% Analysis Date = 07/09/14 Pct Recovery = 86% Analysis Date = 07/09/14 Pct Recovery = 86% Analysis Date = 07/04/14 Pct Recovery = 86% Analysis Date = 07/04/14 Pct Recovery = 86% Analysis Date = 06/30/14 Pct Recovery = 85% Analysis Date = 06/30/14 Pct Recovery = 85% Analysis Date = 06/25/14 Pct Recovery = 85% Analysis Date = 06/25/14 Pct Recovery = 85% Analysis Date = 06/20/14 Pct Recovery = 85% Analysis Date = 06/20/14 Pct Recovery = 85% Analysis Date = 06/15/14 Pct Recovery = 85% Analysis Date = 06/15/14 Pct Recovery = 85% Analysis Date = 06/10/14 Pct Recovery = 84% Analysis Date = 06/10/14 Pct Recovery = 84% Analysis Date = 06/05/14 Pct Recovery = 84% Analysis Date = 06/05/14 Pct Recovery = 84% Analysis Date = 05/31/14 Pct Recovery = 84% Analysis Date = 05/31/14 Pct Recovery = 84% Analysis Date = 05/26/14 Pct Recovery = 83% Analysis Date = 05/26/14 Pct Recovery = 83% Analysis Date = 05/21/14 Pct Recovery = 83% Analysis Date = 05/21/14 Pct Recovery = 83% Analysis Date = 05/17/14 Pct Recovery = 83% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
LORAZEPAM

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 49 106% 27% 104% 19%
Total 49 106% 27% 104% 19%

Sample Statistics
LORAZEPAM

Characteristic N % % Basis
Plotted 49 96% Spiked
Estimated Values 28 55% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 2 4% Spiked
Spiked 51 .  
False Negatives 0 0% 0 out of 51
Not Spiked 64 .  
False Positives 0 0% 0 out of 64

BQS OBSP Determination:
MEPROBAMATE
METHOD: 2440 , TESTIDCODE: 67464LCM56
Open Data Set

Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 95% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 93% Analysis Date = 11/24/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 89% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 80 µl & Abs 051315: 80 µl Pct Recovery = 103% Analysis Date = 10/01/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 114% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 81% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 84% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 94% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 93% Analysis Date = 11/18/16 SpikeMix = ERA 04281604: 80 µl & ERA 04281603: 80 µl Pct Recovery = 82% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & ERA 04281604: 80 µl Pct Recovery = 85% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 79% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 80% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-04: 15 µl & Abs 041814: 15 µl Pct Recovery = 85% Analysis Date = 02/06/15 SpikeMix = Abs 041814: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 89% Analysis Date = 07/12/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 79% Analysis Date = 06/22/14 SpikeMix = Abs 041814: 60 µl & Abs 041614: 60 µl Pct Recovery = 95% Analysis Date = 05/21/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 88% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 89% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 79% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-07A: 40 µl & Abs 051315: 40 µl Pct Recovery = 84% Analysis Date = 07/31/15 SpikeMix = Abs 051315: 40 µl & Abs 052215: 40 µl Pct Recovery = 86% Analysis Date = 07/30/15 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 93% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 109% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 118% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 102% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 96% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 97% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 102% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 75% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 76% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 78% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 68% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 86% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 88% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 78% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 79% Analysis Date = 04/10/15 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 80% Analysis Date = 11/04/14 SpikeMix = Abs 041814: 8 µl & ERA 0318-14-02: 8 µl Pct Recovery = 85% Analysis Date = 10/11/14 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 77% Analysis Date = 10/10/14 SpikeMix = Abs 041714: 30 µl & Abs 041814: 30 µl Pct Recovery = 83% Analysis Date = 10/10/14 SpikeMix = Abs 041814: 30 µl & ERA 0318-14-02: 30 µl Pct Recovery = 78% Analysis Date = 07/13/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 85% Analysis Date = 05/30/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 93% Analysis Date = 02/23/16 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 72% Analysis Date = 08/11/15 SpikeMix = Abs 050115: 20 µl & Abs 051315: 20 µl Pct Recovery = 57% Analysis Date = 06/26/15 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 83% Analysis Date = 06/09/15 SpikeMix = Abs 051315: 20 µl & Abs 050115: 20 µl Pct Recovery = 65% Analysis Date = 04/09/16 SpikeMix = Abs 051315: 10 µl & ERA 0406-15-09: 10 µl Pct Recovery = 68% Analysis Date = 04/09/16 SpikeMix = Abs 051315: 10 µl & ERA 0406-15-09: 10 µl Pct Recovery = 104% Analysis Date = 01/18/17 Pct Recovery = 96% Analysis Date = 01/14/17 Pct Recovery = 96% Analysis Date = 01/14/17 Pct Recovery = 96% Analysis Date = 01/09/17 Pct Recovery = 96% Analysis Date = 01/09/17 Pct Recovery = 96% Analysis Date = 01/04/17 Pct Recovery = 95% Analysis Date = 01/04/17 Pct Recovery = 95% Analysis Date = 12/30/16 Pct Recovery = 95% Analysis Date = 12/30/16 Pct Recovery = 95% Analysis Date = 12/25/16 Pct Recovery = 95% Analysis Date = 12/25/16 Pct Recovery = 95% Analysis Date = 12/20/16 Pct Recovery = 94% Analysis Date = 12/20/16 Pct Recovery = 94% Analysis Date = 12/15/16 Pct Recovery = 94% Analysis Date = 12/15/16 Pct Recovery = 94% Analysis Date = 12/11/16 Pct Recovery = 93% Analysis Date = 12/11/16 Pct Recovery = 93% Analysis Date = 12/06/16 Pct Recovery = 93% Analysis Date = 12/06/16 Pct Recovery = 93% Analysis Date = 12/01/16 Pct Recovery = 93% Analysis Date = 12/01/16 Pct Recovery = 93% Analysis Date = 11/26/16 Pct Recovery = 92% Analysis Date = 11/26/16 Pct Recovery = 92% Analysis Date = 11/21/16 Pct Recovery = 92% Analysis Date = 11/21/16 Pct Recovery = 92% Analysis Date = 11/16/16 Pct Recovery = 91% Analysis Date = 11/16/16 Pct Recovery = 91% Analysis Date = 11/11/16 Pct Recovery = 91% Analysis Date = 11/11/16 Pct Recovery = 91% Analysis Date = 11/06/16 Pct Recovery = 91% Analysis Date = 11/06/16 Pct Recovery = 91% Analysis Date = 11/02/16 Pct Recovery = 90% Analysis Date = 11/02/16 Pct Recovery = 90% Analysis Date = 10/28/16 Pct Recovery = 90% Analysis Date = 10/28/16 Pct Recovery = 90% Analysis Date = 10/23/16 Pct Recovery = 90% Analysis Date = 10/23/16 Pct Recovery = 90% Analysis Date = 10/18/16 Pct Recovery = 89% Analysis Date = 10/18/16 Pct Recovery = 89% Analysis Date = 10/13/16 Pct Recovery = 89% Analysis Date = 10/13/16 Pct Recovery = 89% Analysis Date = 10/08/16 Pct Recovery = 89% Analysis Date = 10/08/16 Pct Recovery = 89% Analysis Date = 10/03/16 Pct Recovery = 88% Analysis Date = 10/03/16 Pct Recovery = 88% Analysis Date = 09/28/16 Pct Recovery = 88% Analysis Date = 09/28/16 Pct Recovery = 88% Analysis Date = 09/24/16 Pct Recovery = 88% Analysis Date = 09/24/16 Pct Recovery = 88% Analysis Date = 09/19/16 Pct Recovery = 87% Analysis Date = 09/19/16 Pct Recovery = 87% Analysis Date = 09/14/16 Pct Recovery = 87% Analysis Date = 09/14/16 Pct Recovery = 87% Analysis Date = 09/09/16 Pct Recovery = 87% Analysis Date = 09/09/16 Pct Recovery = 87% Analysis Date = 09/04/16 Pct Recovery = 86% Analysis Date = 09/04/16 Pct Recovery = 86% Analysis Date = 08/30/16 Pct Recovery = 86% Analysis Date = 08/30/16 Pct Recovery = 86% Analysis Date = 08/25/16 Pct Recovery = 86% Analysis Date = 08/25/16 Pct Recovery = 86% Analysis Date = 08/21/16 Pct Recovery = 85% Analysis Date = 08/21/16 Pct Recovery = 85% Analysis Date = 08/16/16 Pct Recovery = 85% Analysis Date = 08/16/16 Pct Recovery = 85% Analysis Date = 08/11/16 Pct Recovery = 85% Analysis Date = 08/11/16 Pct Recovery = 85% Analysis Date = 08/06/16 Pct Recovery = 85% Analysis Date = 08/06/16 Pct Recovery = 85% Analysis Date = 08/01/16 Pct Recovery = 85% Analysis Date = 08/01/16 Pct Recovery = 85% Analysis Date = 07/27/16 Pct Recovery = 85% Analysis Date = 07/27/16 Pct Recovery = 85% Analysis Date = 07/22/16 Pct Recovery = 85% Analysis Date = 07/22/16 Pct Recovery = 85% Analysis Date = 07/17/16 Pct Recovery = 85% Analysis Date = 07/17/16 Pct Recovery = 85% Analysis Date = 07/13/16 Pct Recovery = 85% Analysis Date = 07/13/16 Pct Recovery = 85% Analysis Date = 07/08/16 Pct Recovery = 85% Analysis Date = 07/08/16 Pct Recovery = 85% Analysis Date = 07/03/16 Pct Recovery = 85% Analysis Date = 07/03/16 Pct Recovery = 85% Analysis Date = 06/28/16 Pct Recovery = 85% Analysis Date = 06/28/16 Pct Recovery = 85% Analysis Date = 06/23/16 Pct Recovery = 84% Analysis Date = 06/23/16 Pct Recovery = 84% Analysis Date = 06/18/16 Pct Recovery = 84% Analysis Date = 06/18/16 Pct Recovery = 84% Analysis Date = 06/13/16 Pct Recovery = 84% Analysis Date = 06/13/16 Pct Recovery = 84% Analysis Date = 06/08/16 Pct Recovery = 84% Analysis Date = 06/08/16 Pct Recovery = 84% Analysis Date = 06/04/16 Pct Recovery = 84% Analysis Date = 06/04/16 Pct Recovery = 84% Analysis Date = 05/30/16 Pct Recovery = 84% Analysis Date = 05/30/16 Pct Recovery = 84% Analysis Date = 05/25/16 Pct Recovery = 84% Analysis Date = 05/25/16 Pct Recovery = 84% Analysis Date = 05/20/16 Pct Recovery = 84% Analysis Date = 05/20/16 Pct Recovery = 84% Analysis Date = 05/15/16 Pct Recovery = 84% Analysis Date = 05/15/16 Pct Recovery = 84% Analysis Date = 05/10/16 Pct Recovery = 84% Analysis Date = 05/10/16 Pct Recovery = 84% Analysis Date = 05/05/16 Pct Recovery = 84% Analysis Date = 05/05/16 Pct Recovery = 84% Analysis Date = 05/01/16 Pct Recovery = 84% Analysis Date = 05/01/16 Pct Recovery = 84% Analysis Date = 04/26/16 Pct Recovery = 84% Analysis Date = 04/26/16 Pct Recovery = 84% Analysis Date = 04/21/16 Pct Recovery = 84% Analysis Date = 04/21/16 Pct Recovery = 84% Analysis Date = 04/16/16 Pct Recovery = 84% Analysis Date = 04/16/16 Pct Recovery = 84% Analysis Date = 04/11/16 Pct Recovery = 84% Analysis Date = 04/11/16 Pct Recovery = 84% Analysis Date = 04/06/16 Pct Recovery = 84% Analysis Date = 04/06/16 Pct Recovery = 84% Analysis Date = 04/01/16 Pct Recovery = 84% Analysis Date = 04/01/16 Pct Recovery = 84% Analysis Date = 03/27/16 Pct Recovery = 84% Analysis Date = 03/27/16 Pct Recovery = 84% Analysis Date = 03/23/16 Pct Recovery = 84% Analysis Date = 03/23/16 Pct Recovery = 84% Analysis Date = 03/18/16 Pct Recovery = 84% Analysis Date = 03/18/16 Pct Recovery = 84% Analysis Date = 03/13/16 Pct Recovery = 84% Analysis Date = 03/13/16 Pct Recovery = 84% Analysis Date = 03/08/16 Pct Recovery = 84% Analysis Date = 03/08/16 Pct Recovery = 84% Analysis Date = 03/03/16 Pct Recovery = 84% Analysis Date = 03/03/16 Pct Recovery = 84% Analysis Date = 02/27/16 Pct Recovery = 84% Analysis Date = 02/27/16 Pct Recovery = 84% Analysis Date = 02/22/16 Pct Recovery = 84% Analysis Date = 02/22/16 Pct Recovery = 84% Analysis Date = 02/17/16 Pct Recovery = 84% Analysis Date = 02/17/16 Pct Recovery = 84% Analysis Date = 02/13/16 Pct Recovery = 84% Analysis Date = 02/13/16 Pct Recovery = 84% Analysis Date = 02/08/16 Pct Recovery = 84% Analysis Date = 02/08/16 Pct Recovery = 84% Analysis Date = 02/03/16 Pct Recovery = 84% Analysis Date = 02/03/16 Pct Recovery = 84% Analysis Date = 01/29/16 Pct Recovery = 84% Analysis Date = 01/29/16 Pct Recovery = 84% Analysis Date = 01/24/16 Pct Recovery = 84% Analysis Date = 01/24/16 Pct Recovery = 84% Analysis Date = 01/19/16 Pct Recovery = 84% Analysis Date = 01/19/16 Pct Recovery = 84% Analysis Date = 01/14/16 Pct Recovery = 84% Analysis Date = 01/14/16 Pct Recovery = 84% Analysis Date = 01/10/16 Pct Recovery = 84% Analysis Date = 01/10/16 Pct Recovery = 84% Analysis Date = 01/05/16 Pct Recovery = 84% Analysis Date = 01/05/16 Pct Recovery = 84% Analysis Date = 12/31/15 Pct Recovery = 84% Analysis Date = 12/31/15 Pct Recovery = 84% Analysis Date = 12/26/15 Pct Recovery = 85% Analysis Date = 12/26/15 Pct Recovery = 85% Analysis Date = 12/21/15 Pct Recovery = 85% Analysis Date = 12/21/15 Pct Recovery = 85% Analysis Date = 12/16/15 Pct Recovery = 85% Analysis Date = 12/16/15 Pct Recovery = 85% Analysis Date = 12/11/15 Pct Recovery = 85% Analysis Date = 12/11/15 Pct Recovery = 85% Analysis Date = 12/06/15 Pct Recovery = 85% Analysis Date = 12/06/15 Pct Recovery = 85% Analysis Date = 12/02/15 Pct Recovery = 85% Analysis Date = 12/02/15 Pct Recovery = 85% Analysis Date = 11/27/15 Pct Recovery = 85% Analysis Date = 11/27/15 Pct Recovery = 85% Analysis Date = 11/22/15 Pct Recovery = 85% Analysis Date = 11/22/15 Pct Recovery = 85% Analysis Date = 11/17/15 Pct Recovery = 85% Analysis Date = 11/17/15 Pct Recovery = 85% Analysis Date = 11/12/15 Pct Recovery = 85% Analysis Date = 11/12/15 Pct Recovery = 85% Analysis Date = 11/07/15 Pct Recovery = 85% Analysis Date = 11/07/15 Pct Recovery = 85% Analysis Date = 11/02/15 Pct Recovery = 85% Analysis Date = 11/02/15 Pct Recovery = 85% Analysis Date = 10/28/15 Pct Recovery = 85% Analysis Date = 10/28/15 Pct Recovery = 85% Analysis Date = 10/24/15 Pct Recovery = 85% Analysis Date = 10/24/15 Pct Recovery = 85% Analysis Date = 10/19/15 Pct Recovery = 85% Analysis Date = 10/19/15 Pct Recovery = 85% Analysis Date = 10/14/15 Pct Recovery = 85% Analysis Date = 10/14/15 Pct Recovery = 85% Analysis Date = 10/09/15 Pct Recovery = 85% Analysis Date = 10/09/15 Pct Recovery = 85% Analysis Date = 10/04/15 Pct Recovery = 85% Analysis Date = 10/04/15 Pct Recovery = 85% Analysis Date = 09/29/15 Pct Recovery = 85% Analysis Date = 09/29/15 Pct Recovery = 85% Analysis Date = 09/24/15 Pct Recovery = 85% Analysis Date = 09/24/15 Pct Recovery = 85% Analysis Date = 09/19/15 Pct Recovery = 85% Analysis Date = 09/19/15 Pct Recovery = 85% Analysis Date = 09/15/15 Pct Recovery = 85% Analysis Date = 09/15/15 Pct Recovery = 85% Analysis Date = 09/10/15 Pct Recovery = 85% Analysis Date = 09/10/15 Pct Recovery = 85% Analysis Date = 09/05/15 Pct Recovery = 85% Analysis Date = 09/05/15 Pct Recovery = 85% Analysis Date = 08/31/15 Pct Recovery = 85% Analysis Date = 08/31/15 Pct Recovery = 85% Analysis Date = 08/26/15 Pct Recovery = 85% Analysis Date = 08/26/15 Pct Recovery = 85% Analysis Date = 08/21/15 Pct Recovery = 85% Analysis Date = 08/21/15 Pct Recovery = 85% Analysis Date = 08/16/15 Pct Recovery = 85% Analysis Date = 08/16/15 Pct Recovery = 85% Analysis Date = 08/12/15 Pct Recovery = 85% Analysis Date = 08/12/15 Pct Recovery = 85% Analysis Date = 08/07/15 Pct Recovery = 85% Analysis Date = 08/07/15 Pct Recovery = 85% Analysis Date = 08/02/15 Pct Recovery = 85% Analysis Date = 08/02/15 Pct Recovery = 85% Analysis Date = 07/28/15 Pct Recovery = 85% Analysis Date = 07/28/15 Pct Recovery = 85% Analysis Date = 07/23/15 Pct Recovery = 85% Analysis Date = 07/23/15 Pct Recovery = 85% Analysis Date = 07/18/15 Pct Recovery = 85% Analysis Date = 07/18/15 Pct Recovery = 85% Analysis Date = 07/13/15 Pct Recovery = 84% Analysis Date = 07/13/15 Pct Recovery = 84% Analysis Date = 07/08/15 Pct Recovery = 84% Analysis Date = 07/08/15 Pct Recovery = 84% Analysis Date = 07/04/15 Pct Recovery = 84% Analysis Date = 07/04/15 Pct Recovery = 84% Analysis Date = 06/29/15 Pct Recovery = 84% Analysis Date = 06/29/15 Pct Recovery = 84% Analysis Date = 06/24/15 Pct Recovery = 84% Analysis Date = 06/24/15 Pct Recovery = 84% Analysis Date = 06/19/15 Pct Recovery = 84% Analysis Date = 06/19/15 Pct Recovery = 84% Analysis Date = 06/14/15 Pct Recovery = 84% Analysis Date = 06/14/15 Pct Recovery = 84% Analysis Date = 06/09/15 Pct Recovery = 84% Analysis Date = 06/09/15 Pct Recovery = 84% Analysis Date = 06/04/15 Pct Recovery = 84% Analysis Date = 06/04/15 Pct Recovery = 84% Analysis Date = 05/30/15 Pct Recovery = 84% Analysis Date = 05/30/15 Pct Recovery = 84% Analysis Date = 05/26/15 Pct Recovery = 84% Analysis Date = 05/26/15 Pct Recovery = 84% Analysis Date = 05/21/15 Pct Recovery = 84% Analysis Date = 05/21/15 Pct Recovery = 84% Analysis Date = 05/16/15 Pct Recovery = 84% Analysis Date = 05/16/15 Pct Recovery = 84% Analysis Date = 05/11/15 Pct Recovery = 84% Analysis Date = 05/11/15 Pct Recovery = 84% Analysis Date = 05/06/15 Pct Recovery = 84% Analysis Date = 05/06/15 Pct Recovery = 84% Analysis Date = 05/01/15 Pct Recovery = 84% Analysis Date = 05/01/15 Pct Recovery = 84% Analysis Date = 04/26/15 Pct Recovery = 84% Analysis Date = 04/26/15 Pct Recovery = 84% Analysis Date = 04/22/15 Pct Recovery = 84% Analysis Date = 04/22/15 Pct Recovery = 84% Analysis Date = 04/17/15 Pct Recovery = 84% Analysis Date = 04/17/15 Pct Recovery = 84% Analysis Date = 04/12/15 Pct Recovery = 84% Analysis Date = 04/12/15 Pct Recovery = 84% Analysis Date = 04/07/15 Pct Recovery = 84% Analysis Date = 04/07/15 Pct Recovery = 84% Analysis Date = 04/02/15 Pct Recovery = 84% Analysis Date = 04/02/15 Pct Recovery = 84% Analysis Date = 03/28/15 Pct Recovery = 84% Analysis Date = 03/28/15 Pct Recovery = 84% Analysis Date = 03/23/15 Pct Recovery = 84% Analysis Date = 03/23/15 Pct Recovery = 84% Analysis Date = 03/18/15 Pct Recovery = 84% Analysis Date = 03/18/15 Pct Recovery = 84% Analysis Date = 03/14/15 Pct Recovery = 84% Analysis Date = 03/14/15 Pct Recovery = 84% Analysis Date = 03/09/15 Pct Recovery = 84% Analysis Date = 03/09/15 Pct Recovery = 84% Analysis Date = 03/04/15 Pct Recovery = 84% Analysis Date = 03/04/15 Pct Recovery = 84% Analysis Date = 02/27/15 Pct Recovery = 84% Analysis Date = 02/27/15 Pct Recovery = 84% Analysis Date = 02/22/15 Pct Recovery = 84% Analysis Date = 02/22/15 Pct Recovery = 84% Analysis Date = 02/17/15 Pct Recovery = 84% Analysis Date = 02/17/15 Pct Recovery = 84% Analysis Date = 02/12/15 Pct Recovery = 84% Analysis Date = 02/12/15 Pct Recovery = 84% Analysis Date = 02/07/15 Pct Recovery = 85% Analysis Date = 02/07/15 Pct Recovery = 85% Analysis Date = 02/03/15 Pct Recovery = 85% Analysis Date = 02/03/15 Pct Recovery = 85% Analysis Date = 01/29/15 Pct Recovery = 85% Analysis Date = 01/29/15 Pct Recovery = 85% Analysis Date = 01/24/15 Pct Recovery = 85% Analysis Date = 01/24/15 Pct Recovery = 85% Analysis Date = 01/19/15 Pct Recovery = 85% Analysis Date = 01/19/15 Pct Recovery = 85% Analysis Date = 01/14/15 Pct Recovery = 85% Analysis Date = 01/14/15 Pct Recovery = 85% Analysis Date = 01/09/15 Pct Recovery = 85% Analysis Date = 01/09/15 Pct Recovery = 85% Analysis Date = 01/04/15 Pct Recovery = 85% Analysis Date = 01/04/15 Pct Recovery = 85% Analysis Date = 12/31/14 Pct Recovery = 85% Analysis Date = 12/31/14 Pct Recovery = 85% Analysis Date = 12/26/14 Pct Recovery = 85% Analysis Date = 12/26/14 Pct Recovery = 85% Analysis Date = 12/21/14 Pct Recovery = 85% Analysis Date = 12/21/14 Pct Recovery = 85% Analysis Date = 12/16/14 Pct Recovery = 85% Analysis Date = 12/16/14 Pct Recovery = 85% Analysis Date = 12/11/14 Pct Recovery = 85% Analysis Date = 12/11/14 Pct Recovery = 85% Analysis Date = 12/06/14 Pct Recovery = 85% Analysis Date = 12/06/14 Pct Recovery = 85% Analysis Date = 12/01/14 Pct Recovery = 85% Analysis Date = 12/01/14 Pct Recovery = 85% Analysis Date = 11/26/14 Pct Recovery = 85% Analysis Date = 11/26/14 Pct Recovery = 85% Analysis Date = 11/22/14 Pct Recovery = 85% Analysis Date = 11/22/14 Pct Recovery = 85% Analysis Date = 11/17/14 Pct Recovery = 85% Analysis Date = 11/17/14 Pct Recovery = 85% Analysis Date = 11/12/14 Pct Recovery = 85% Analysis Date = 11/12/14 Pct Recovery = 85% Analysis Date = 11/07/14 Pct Recovery = 85% Analysis Date = 11/07/14 Pct Recovery = 85% Analysis Date = 11/02/14 Pct Recovery = 85% Analysis Date = 11/02/14 Pct Recovery = 85% Analysis Date = 10/28/14 Pct Recovery = 85% Analysis Date = 10/28/14 Pct Recovery = 85% Analysis Date = 10/23/14 Pct Recovery = 85% Analysis Date = 10/23/14 Pct Recovery = 85% Analysis Date = 10/18/14 Pct Recovery = 85% Analysis Date = 10/18/14 Pct Recovery = 85% Analysis Date = 10/14/14 Pct Recovery = 85% Analysis Date = 10/14/14 Pct Recovery = 85% Analysis Date = 10/09/14 Pct Recovery = 85% Analysis Date = 10/09/14 Pct Recovery = 85% Analysis Date = 10/04/14 Pct Recovery = 85% Analysis Date = 10/04/14 Pct Recovery = 85% Analysis Date = 09/29/14 Pct Recovery = 85% Analysis Date = 09/29/14 Pct Recovery = 85% Analysis Date = 09/24/14 Pct Recovery = 85% Analysis Date = 09/24/14 Pct Recovery = 85% Analysis Date = 09/19/14 Pct Recovery = 85% Analysis Date = 09/19/14 Pct Recovery = 85% Analysis Date = 09/14/14 Pct Recovery = 85% Analysis Date = 09/14/14 Pct Recovery = 85% Analysis Date = 09/10/14 Pct Recovery = 85% Analysis Date = 09/10/14 Pct Recovery = 85% Analysis Date = 09/05/14 Pct Recovery = 85% Analysis Date = 09/05/14 Pct Recovery = 85% Analysis Date = 08/31/14 Pct Recovery = 85% Analysis Date = 08/31/14 Pct Recovery = 85% Analysis Date = 08/26/14 Pct Recovery = 85% Analysis Date = 08/26/14 Pct Recovery = 85% Analysis Date = 08/21/14 Pct Recovery = 85% Analysis Date = 08/21/14 Pct Recovery = 85% Analysis Date = 08/16/14 Pct Recovery = 85% Analysis Date = 08/16/14 Pct Recovery = 85% Analysis Date = 08/11/14 Pct Recovery = 85% Analysis Date = 08/11/14 Pct Recovery = 85% Analysis Date = 08/06/14 Pct Recovery = 85% Analysis Date = 08/06/14 Pct Recovery = 85% Analysis Date = 08/02/14 Pct Recovery = 85% Analysis Date = 08/02/14 Pct Recovery = 85% Analysis Date = 07/28/14 Pct Recovery = 85% Analysis Date = 07/28/14 Pct Recovery = 85% Analysis Date = 07/23/14 Pct Recovery = 85% Analysis Date = 07/23/14 Pct Recovery = 85% Analysis Date = 07/18/14 Pct Recovery = 85% Analysis Date = 07/18/14 Pct Recovery = 85% Analysis Date = 07/13/14 Pct Recovery = 85% Analysis Date = 07/13/14 Pct Recovery = 85% Analysis Date = 07/08/14 Pct Recovery = 85% Analysis Date = 07/08/14 Pct Recovery = 85% Analysis Date = 07/03/14 Pct Recovery = 85% Analysis Date = 07/03/14 Pct Recovery = 85% Analysis Date = 06/28/14 Pct Recovery = 85% Analysis Date = 06/28/14 Pct Recovery = 85% Analysis Date = 06/24/14 Pct Recovery = 85% Analysis Date = 06/24/14 Pct Recovery = 85% Analysis Date = 06/19/14 Pct Recovery = 85% Analysis Date = 06/19/14 Pct Recovery = 85% Analysis Date = 06/14/14 Pct Recovery = 85% Analysis Date = 06/14/14 Pct Recovery = 85% Analysis Date = 06/09/14 Pct Recovery = 85% Analysis Date = 06/09/14 Pct Recovery = 85% Analysis Date = 06/04/14 Pct Recovery = 85% Analysis Date = 06/04/14 Pct Recovery = 85% Analysis Date = 05/30/14 Pct Recovery = 85% Analysis Date = 05/30/14 Pct Recovery = 85% Analysis Date = 05/25/14 Pct Recovery = 85% Analysis Date = 05/25/14 Pct Recovery = 85% Analysis Date = 05/21/14 Pct Recovery = 85% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
MEPROBAMATE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 2 86% 26% 86% 27%
>= Reporting Level 48 86% 12% 85% 11%
Total 50 86% 12% 85% 11%

Sample Statistics
MEPROBAMATE

Characteristic N % % Basis
Plotted 50 100% Spiked
Estimated Values 4 8% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 50 .  
False Negatives 0 0% 0 out of 50
Not Spiked 65 .  
False Positives 0 0% 0 out of 65

BQS OBSP Determination:
METAXALONE
METHOD: 2440 , TESTIDCODE: 67504LCM56
Open Data Set

Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 26% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 20% Analysis Date = 01/17/16 SpikeMix = ERA 0406-15-09: 80 µl & ERA 0406-15-07A: 80 µl Pct Recovery = 20% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 80 µl & Abs 051315: 80 µl Pct Recovery = 25% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 80 µl & ERA 0406-15-08: 80 µl Pct Recovery = 73% Analysis Date = 11/04/15 SpikeMix = Abs 052215: 80 µl & Abs 050115: 80 µl Pct Recovery = 80% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 58% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 60% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 75% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 74% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & ERA 04281604: 80 µl Pct Recovery = 17% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 17% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 16% Analysis Date = 05/07/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 86% Analysis Date = 04/29/15 SpikeMix = ERA 0319-14-05: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 87% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 68% Analysis Date = 01/16/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 80% Analysis Date = 12/07/14 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 57% Analysis Date = 12/06/14 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 48% Analysis Date = 08/28/14 SpikeMix = ERA 0319-14-04: 60 µl & ERA 0319-14-05: 60 µl Pct Recovery = 56% Analysis Date = 07/26/14 SpikeMix = ERA 0319-14-05: 60 µl & ERA 0318-14-02: 60 µl Pct Recovery = 75% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-04: 15 µl & Abs 041814: 15 µl Pct Recovery = 61% Analysis Date = 02/06/15 SpikeMix = Abs 041814: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 73% Analysis Date = 07/12/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 80% Analysis Date = 06/22/14 SpikeMix = Abs 041814: 60 µl & Abs 041614: 60 µl Pct Recovery = 100% Analysis Date = 05/21/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 82% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-07A: 40 µl & Abs 051315: 40 µl Pct Recovery = 17% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 69% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 64% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 81% Analysis Date = 02/23/16 SpikeMix = Abs 052215: 40 µl & Abs 050115: 40 µl Pct Recovery = 96% Analysis Date = 07/31/15 SpikeMix = ERA 0406-15-09: 40 µl & Abs 050115: 40 µl Pct Recovery = 81% Analysis Date = 07/30/15 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 71% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 98% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 102% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 79% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 79% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 68% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 64% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 57% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 62% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 71% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 45% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 12% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 13% Analysis Date = 11/04/14 SpikeMix = Abs 041714: 8 µl & ERA 0319-14-05: 8 µl Pct Recovery = 71% Analysis Date = 10/24/14 SpikeMix = ERA 0319-14-05: 8 µl & Abs 041614: 8 µl Pct Recovery = 79% Analysis Date = 04/10/15 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 63% Analysis Date = 11/04/14 SpikeMix = Abs 041814: 8 µl & ERA 0318-14-02: 8 µl Pct Recovery = 73% Analysis Date = 10/11/14 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 46% Analysis Date = 08/30/14 SpikeMix = ERA 0318-14-02: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 78% Analysis Date = 08/16/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 42% Analysis Date = 07/13/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 62% Analysis Date = 10/10/14 SpikeMix = Abs 041714: 30 µl & Abs 041814: 30 µl Pct Recovery = 63% Analysis Date = 10/10/14 SpikeMix = Abs 041814: 30 µl & ERA 0318-14-02: 30 µl Pct Recovery = 44% Analysis Date = 07/13/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 68% Analysis Date = 05/30/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 69% Analysis Date = 04/23/14 SpikeMix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.2: 20 µl Pct Recovery = 70% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 58% Analysis Date = 04/27/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 30% Analysis Date = 11/25/15 SpikeMix = Abs 050115: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 72% Analysis Date = 11/24/15 SpikeMix = ERA 0406-15-09: 20 µl & Abs 050115: 20 µl Pct Recovery = 81% Analysis Date = 08/27/15 SpikeMix = Abs 052215: 20 µl & Abs 050115: 20 µl Pct Recovery = 74% Analysis Date = 08/11/15 SpikeMix = Abs 050115: 20 µl & Abs 051315: 20 µl Pct Recovery = 56% Analysis Date = 07/09/15 SpikeMix = Abs 050115: 20 µl & Abs 052215: 20 µl Pct Recovery = 90% Analysis Date = 06/09/15 SpikeMix = Abs 051315: 20 µl & Abs 050115: 20 µl Pct Recovery = 65% Analysis Date = 01/18/17 Pct Recovery = 48% Analysis Date = 01/13/17 Pct Recovery = 49% Analysis Date = 01/13/17 Pct Recovery = 49% Analysis Date = 01/08/17 Pct Recovery = 49% Analysis Date = 01/08/17 Pct Recovery = 49% Analysis Date = 01/03/17 Pct Recovery = 49% Analysis Date = 01/03/17 Pct Recovery = 49% Analysis Date = 12/29/16 Pct Recovery = 49% Analysis Date = 12/29/16 Pct Recovery = 49% Analysis Date = 12/24/16 Pct Recovery = 49% Analysis Date = 12/24/16 Pct Recovery = 49% Analysis Date = 12/19/16 Pct Recovery = 50% Analysis Date = 12/19/16 Pct Recovery = 50% Analysis Date = 12/14/16 Pct Recovery = 50% Analysis Date = 12/14/16 Pct Recovery = 50% Analysis Date = 12/09/16 Pct Recovery = 50% Analysis Date = 12/09/16 Pct Recovery = 50% Analysis Date = 12/04/16 Pct Recovery = 50% Analysis Date = 12/04/16 Pct Recovery = 50% Analysis Date = 11/29/16 Pct Recovery = 51% Analysis Date = 11/29/16 Pct Recovery = 51% Analysis Date = 11/24/16 Pct Recovery = 51% Analysis Date = 11/24/16 Pct Recovery = 51% Analysis Date = 11/19/16 Pct Recovery = 51% Analysis Date = 11/19/16 Pct Recovery = 51% Analysis Date = 11/14/16 Pct Recovery = 51% Analysis Date = 11/14/16 Pct Recovery = 51% Analysis Date = 11/09/16 Pct Recovery = 51% Analysis Date = 11/09/16 Pct Recovery = 51% Analysis Date = 11/04/16 Pct Recovery = 52% Analysis Date = 11/04/16 Pct Recovery = 52% Analysis Date = 10/30/16 Pct Recovery = 52% Analysis Date = 10/30/16 Pct Recovery = 52% Analysis Date = 10/25/16 Pct Recovery = 52% Analysis Date = 10/25/16 Pct Recovery = 52% Analysis Date = 10/20/16 Pct Recovery = 52% Analysis Date = 10/20/16 Pct Recovery = 52% Analysis Date = 10/15/16 Pct Recovery = 52% Analysis Date = 10/15/16 Pct Recovery = 52% Analysis Date = 10/10/16 Pct Recovery = 53% Analysis Date = 10/10/16 Pct Recovery = 53% Analysis Date = 10/05/16 Pct Recovery = 53% Analysis Date = 10/05/16 Pct Recovery = 53% Analysis Date = 09/30/16 Pct Recovery = 53% Analysis Date = 09/30/16 Pct Recovery = 53% Analysis Date = 09/25/16 Pct Recovery = 53% Analysis Date = 09/25/16 Pct Recovery = 53% Analysis Date = 09/20/16 Pct Recovery = 53% Analysis Date = 09/20/16 Pct Recovery = 53% Analysis Date = 09/15/16 Pct Recovery = 54% Analysis Date = 09/15/16 Pct Recovery = 54% Analysis Date = 09/10/16 Pct Recovery = 54% Analysis Date = 09/10/16 Pct Recovery = 54% Analysis Date = 09/05/16 Pct Recovery = 54% Analysis Date = 09/05/16 Pct Recovery = 54% Analysis Date = 08/31/16 Pct Recovery = 54% Analysis Date = 08/31/16 Pct Recovery = 54% Analysis Date = 08/26/16 Pct Recovery = 54% Analysis Date = 08/26/16 Pct Recovery = 54% Analysis Date = 08/21/16 Pct Recovery = 55% Analysis Date = 08/21/16 Pct Recovery = 55% Analysis Date = 08/16/16 Pct Recovery = 55% Analysis Date = 08/16/16 Pct Recovery = 55% Analysis Date = 08/11/16 Pct Recovery = 55% Analysis Date = 08/11/16 Pct Recovery = 55% Analysis Date = 08/06/16 Pct Recovery = 55% Analysis Date = 08/06/16 Pct Recovery = 55% Analysis Date = 08/01/16 Pct Recovery = 55% Analysis Date = 08/01/16 Pct Recovery = 55% Analysis Date = 07/27/16 Pct Recovery = 56% Analysis Date = 07/27/16 Pct Recovery = 56% Analysis Date = 07/22/16 Pct Recovery = 56% Analysis Date = 07/22/16 Pct Recovery = 56% Analysis Date = 07/17/16 Pct Recovery = 56% Analysis Date = 07/17/16 Pct Recovery = 56% Analysis Date = 07/12/16 Pct Recovery = 56% Analysis Date = 07/12/16 Pct Recovery = 56% Analysis Date = 07/07/16 Pct Recovery = 56% Analysis Date = 07/07/16 Pct Recovery = 56% Analysis Date = 07/02/16 Pct Recovery = 56% Analysis Date = 07/02/16 Pct Recovery = 56% Analysis Date = 06/27/16 Pct Recovery = 57% Analysis Date = 06/27/16 Pct Recovery = 57% Analysis Date = 06/22/16 Pct Recovery = 57% Analysis Date = 06/22/16 Pct Recovery = 57% Analysis Date = 06/17/16 Pct Recovery = 57% Analysis Date = 06/17/16 Pct Recovery = 57% Analysis Date = 06/12/16 Pct Recovery = 57% Analysis Date = 06/12/16 Pct Recovery = 57% Analysis Date = 06/07/16 Pct Recovery = 57% Analysis Date = 06/07/16 Pct Recovery = 57% Analysis Date = 06/02/16 Pct Recovery = 57% Analysis Date = 06/02/16 Pct Recovery = 57% Analysis Date = 05/28/16 Pct Recovery = 58% Analysis Date = 05/28/16 Pct Recovery = 58% Analysis Date = 05/23/16 Pct Recovery = 58% Analysis Date = 05/23/16 Pct Recovery = 58% Analysis Date = 05/18/16 Pct Recovery = 58% Analysis Date = 05/18/16 Pct Recovery = 58% Analysis Date = 05/13/16 Pct Recovery = 58% Analysis Date = 05/13/16 Pct Recovery = 58% Analysis Date = 05/08/16 Pct Recovery = 58% Analysis Date = 05/08/16 Pct Recovery = 58% Analysis Date = 05/03/16 Pct Recovery = 59% Analysis Date = 05/03/16 Pct Recovery = 59% Analysis Date = 04/28/16 Pct Recovery = 59% Analysis Date = 04/28/16 Pct Recovery = 59% Analysis Date = 04/23/16 Pct Recovery = 59% Analysis Date = 04/23/16 Pct Recovery = 59% Analysis Date = 04/18/16 Pct Recovery = 59% Analysis Date = 04/18/16 Pct Recovery = 59% Analysis Date = 04/13/16 Pct Recovery = 59% Analysis Date = 04/13/16 Pct Recovery = 59% Analysis Date = 04/08/16 Pct Recovery = 59% Analysis Date = 04/08/16 Pct Recovery = 59% Analysis Date = 04/03/16 Pct Recovery = 60% Analysis Date = 04/03/16 Pct Recovery = 60% Analysis Date = 03/29/16 Pct Recovery = 60% Analysis Date = 03/29/16 Pct Recovery = 60% Analysis Date = 03/24/16 Pct Recovery = 60% Analysis Date = 03/24/16 Pct Recovery = 60% Analysis Date = 03/19/16 Pct Recovery = 60% Analysis Date = 03/19/16 Pct Recovery = 60% Analysis Date = 03/14/16 Pct Recovery = 60% Analysis Date = 03/14/16 Pct Recovery = 60% Analysis Date = 03/09/16 Pct Recovery = 60% Analysis Date = 03/09/16 Pct Recovery = 60% Analysis Date = 03/04/16 Pct Recovery = 61% Analysis Date = 03/04/16 Pct Recovery = 61% Analysis Date = 02/28/16 Pct Recovery = 61% Analysis Date = 02/28/16 Pct Recovery = 61% Analysis Date = 02/23/16 Pct Recovery = 61% Analysis Date = 02/23/16 Pct Recovery = 61% Analysis Date = 02/18/16 Pct Recovery = 61% Analysis Date = 02/18/16 Pct Recovery = 61% Analysis Date = 02/13/16 Pct Recovery = 61% Analysis Date = 02/13/16 Pct Recovery = 61% Analysis Date = 02/08/16 Pct Recovery = 61% Analysis Date = 02/08/16 Pct Recovery = 61% Analysis Date = 02/03/16 Pct Recovery = 62% Analysis Date = 02/03/16 Pct Recovery = 62% Analysis Date = 01/29/16 Pct Recovery = 62% Analysis Date = 01/29/16 Pct Recovery = 62% Analysis Date = 01/24/16 Pct Recovery = 62% Analysis Date = 01/24/16 Pct Recovery = 62% Analysis Date = 01/19/16 Pct Recovery = 62% Analysis Date = 01/19/16 Pct Recovery = 62% Analysis Date = 01/14/16 Pct Recovery = 62% Analysis Date = 01/14/16 Pct Recovery = 62% Analysis Date = 01/09/16 Pct Recovery = 62% Analysis Date = 01/09/16 Pct Recovery = 62% Analysis Date = 01/04/16 Pct Recovery = 63% Analysis Date = 01/04/16 Pct Recovery = 63% Analysis Date = 12/30/15 Pct Recovery = 63% Analysis Date = 12/30/15 Pct Recovery = 63% Analysis Date = 12/25/15 Pct Recovery = 63% Analysis Date = 12/25/15 Pct Recovery = 63% Analysis Date = 12/20/15 Pct Recovery = 63% Analysis Date = 12/20/15 Pct Recovery = 63% Analysis Date = 12/15/15 Pct Recovery = 63% Analysis Date = 12/15/15 Pct Recovery = 63% Analysis Date = 12/10/15 Pct Recovery = 63% Analysis Date = 12/10/15 Pct Recovery = 63% Analysis Date = 12/05/15 Pct Recovery = 64% Analysis Date = 12/05/15 Pct Recovery = 64% Analysis Date = 11/30/15 Pct Recovery = 64% Analysis Date = 11/30/15 Pct Recovery = 64% Analysis Date = 11/25/15 Pct Recovery = 64% Analysis Date = 11/25/15 Pct Recovery = 64% Analysis Date = 11/20/15 Pct Recovery = 64% Analysis Date = 11/20/15 Pct Recovery = 64% Analysis Date = 11/15/15 Pct Recovery = 64% Analysis Date = 11/15/15 Pct Recovery = 64% Analysis Date = 11/10/15 Pct Recovery = 65% Analysis Date = 11/10/15 Pct Recovery = 65% Analysis Date = 11/05/15 Pct Recovery = 65% Analysis Date = 11/05/15 Pct Recovery = 65% Analysis Date = 10/31/15 Pct Recovery = 65% Analysis Date = 10/31/15 Pct Recovery = 65% Analysis Date = 10/26/15 Pct Recovery = 65% Analysis Date = 10/26/15 Pct Recovery = 65% Analysis Date = 10/21/15 Pct Recovery = 65% Analysis Date = 10/21/15 Pct Recovery = 65% Analysis Date = 10/16/15 Pct Recovery = 65% Analysis Date = 10/16/15 Pct Recovery = 65% Analysis Date = 10/11/15 Pct Recovery = 66% Analysis Date = 10/11/15 Pct Recovery = 66% Analysis Date = 10/06/15 Pct Recovery = 66% Analysis Date = 10/06/15 Pct Recovery = 66% Analysis Date = 10/01/15 Pct Recovery = 66% Analysis Date = 10/01/15 Pct Recovery = 66% Analysis Date = 09/26/15 Pct Recovery = 66% Analysis Date = 09/26/15 Pct Recovery = 66% Analysis Date = 09/21/15 Pct Recovery = 66% Analysis Date = 09/21/15 Pct Recovery = 66% Analysis Date = 09/16/15 Pct Recovery = 66% Analysis Date = 09/16/15 Pct Recovery = 66% Analysis Date = 09/11/15 Pct Recovery = 66% Analysis Date = 09/11/15 Pct Recovery = 66% Analysis Date = 09/05/15 Pct Recovery = 66% Analysis Date = 09/05/15 Pct Recovery = 66% Analysis Date = 08/31/15 Pct Recovery = 66% Analysis Date = 08/31/15 Pct Recovery = 66% Analysis Date = 08/26/15 Pct Recovery = 66% Analysis Date = 08/26/15 Pct Recovery = 66% Analysis Date = 08/21/15 Pct Recovery = 66% Analysis Date = 08/21/15 Pct Recovery = 66% Analysis Date = 08/16/15 Pct Recovery = 66% Analysis Date = 08/16/15 Pct Recovery = 66% Analysis Date = 08/11/15 Pct Recovery = 67% Analysis Date = 08/11/15 Pct Recovery = 67% Analysis Date = 08/06/15 Pct Recovery = 67% Analysis Date = 08/06/15 Pct Recovery = 67% Analysis Date = 08/01/15 Pct Recovery = 67% Analysis Date = 08/01/15 Pct Recovery = 67% Analysis Date = 07/27/15 Pct Recovery = 67% Analysis Date = 07/27/15 Pct Recovery = 67% Analysis Date = 07/22/15 Pct Recovery = 67% Analysis Date = 07/22/15 Pct Recovery = 67% Analysis Date = 07/17/15 Pct Recovery = 67% Analysis Date = 07/17/15 Pct Recovery = 67% Analysis Date = 07/12/15 Pct Recovery = 67% Analysis Date = 07/12/15 Pct Recovery = 67% Analysis Date = 07/07/15 Pct Recovery = 67% Analysis Date = 07/07/15 Pct Recovery = 67% Analysis Date = 07/02/15 Pct Recovery = 67% Analysis Date = 07/02/15 Pct Recovery = 67% Analysis Date = 06/27/15 Pct Recovery = 67% Analysis Date = 06/27/15 Pct Recovery = 67% Analysis Date = 06/22/15 Pct Recovery = 67% Analysis Date = 06/22/15 Pct Recovery = 67% Analysis Date = 06/17/15 Pct Recovery = 67% Analysis Date = 06/17/15 Pct Recovery = 67% Analysis Date = 06/12/15 Pct Recovery = 67% Analysis Date = 06/12/15 Pct Recovery = 67% Analysis Date = 06/07/15 Pct Recovery = 67% Analysis Date = 06/07/15 Pct Recovery = 67% Analysis Date = 06/02/15 Pct Recovery = 67% Analysis Date = 06/02/15 Pct Recovery = 67% Analysis Date = 05/28/15 Pct Recovery = 67% Analysis Date = 05/28/15 Pct Recovery = 67% Analysis Date = 05/23/15 Pct Recovery = 67% Analysis Date = 05/23/15 Pct Recovery = 67% Analysis Date = 05/18/15 Pct Recovery = 67% Analysis Date = 05/18/15 Pct Recovery = 67% Analysis Date = 05/13/15 Pct Recovery = 67% Analysis Date = 05/13/15 Pct Recovery = 67% Analysis Date = 05/08/15 Pct Recovery = 67% Analysis Date = 05/08/15 Pct Recovery = 67% Analysis Date = 05/03/15 Pct Recovery = 67% Analysis Date = 05/03/15 Pct Recovery = 67% Analysis Date = 04/28/15 Pct Recovery = 67% Analysis Date = 04/28/15 Pct Recovery = 67% Analysis Date = 04/23/15 Pct Recovery = 68% Analysis Date = 04/23/15 Pct Recovery = 68% Analysis Date = 04/18/15 Pct Recovery = 68% Analysis Date = 04/18/15 Pct Recovery = 68% Analysis Date = 04/13/15 Pct Recovery = 68% Analysis Date = 04/13/15 Pct Recovery = 68% Analysis Date = 04/08/15 Pct Recovery = 68% Analysis Date = 04/08/15 Pct Recovery = 68% Analysis Date = 04/03/15 Pct Recovery = 68% Analysis Date = 04/03/15 Pct Recovery = 68% Analysis Date = 03/29/15 Pct Recovery = 68% Analysis Date = 03/29/15 Pct Recovery = 68% Analysis Date = 03/24/15 Pct Recovery = 68% Analysis Date = 03/24/15 Pct Recovery = 68% Analysis Date = 03/19/15 Pct Recovery = 68% Analysis Date = 03/19/15 Pct Recovery = 68% Analysis Date = 03/14/15 Pct Recovery = 68% Analysis Date = 03/14/15 Pct Recovery = 68% Analysis Date = 03/09/15 Pct Recovery = 68% Analysis Date = 03/09/15 Pct Recovery = 68% Analysis Date = 03/04/15 Pct Recovery = 68% Analysis Date = 03/04/15 Pct Recovery = 68% Analysis Date = 02/27/15 Pct Recovery = 68% Analysis Date = 02/27/15 Pct Recovery = 68% Analysis Date = 02/22/15 Pct Recovery = 68% Analysis Date = 02/22/15 Pct Recovery = 68% Analysis Date = 02/17/15 Pct Recovery = 68% Analysis Date = 02/17/15 Pct Recovery = 68% Analysis Date = 02/12/15 Pct Recovery = 68% Analysis Date = 02/12/15 Pct Recovery = 68% Analysis Date = 02/07/15 Pct Recovery = 68% Analysis Date = 02/07/15 Pct Recovery = 68% Analysis Date = 02/02/15 Pct Recovery = 68% Analysis Date = 02/02/15 Pct Recovery = 68% Analysis Date = 01/28/15 Pct Recovery = 68% Analysis Date = 01/28/15 Pct Recovery = 68% Analysis Date = 01/23/15 Pct Recovery = 68% Analysis Date = 01/23/15 Pct Recovery = 68% Analysis Date = 01/18/15 Pct Recovery = 68% Analysis Date = 01/18/15 Pct Recovery = 68% Analysis Date = 01/13/15 Pct Recovery = 68% Analysis Date = 01/13/15 Pct Recovery = 68% Analysis Date = 01/08/15 Pct Recovery = 68% Analysis Date = 01/08/15 Pct Recovery = 68% Analysis Date = 01/03/15 Pct Recovery = 68% Analysis Date = 01/03/15 Pct Recovery = 68% Analysis Date = 12/29/14 Pct Recovery = 68% Analysis Date = 12/29/14 Pct Recovery = 68% Analysis Date = 12/24/14 Pct Recovery = 68% Analysis Date = 12/24/14 Pct Recovery = 68% Analysis Date = 12/19/14 Pct Recovery = 68% Analysis Date = 12/19/14 Pct Recovery = 68% Analysis Date = 12/14/14 Pct Recovery = 68% Analysis Date = 12/14/14 Pct Recovery = 68% Analysis Date = 12/09/14 Pct Recovery = 68% Analysis Date = 12/09/14 Pct Recovery = 68% Analysis Date = 12/04/14 Pct Recovery = 68% Analysis Date = 12/04/14 Pct Recovery = 68% Analysis Date = 11/29/14 Pct Recovery = 68% Analysis Date = 11/29/14 Pct Recovery = 68% Analysis Date = 11/24/14 Pct Recovery = 68% Analysis Date = 11/24/14 Pct Recovery = 68% Analysis Date = 11/19/14 Pct Recovery = 68% Analysis Date = 11/19/14 Pct Recovery = 68% Analysis Date = 11/14/14 Pct Recovery = 68% Analysis Date = 11/14/14 Pct Recovery = 68% Analysis Date = 11/09/14 Pct Recovery = 68% Analysis Date = 11/09/14 Pct Recovery = 68% Analysis Date = 11/04/14 Pct Recovery = 68% Analysis Date = 11/04/14 Pct Recovery = 68% Analysis Date = 10/30/14 Pct Recovery = 68% Analysis Date = 10/30/14 Pct Recovery = 68% Analysis Date = 10/25/14 Pct Recovery = 68% Analysis Date = 10/25/14 Pct Recovery = 68% Analysis Date = 10/20/14 Pct Recovery = 68% Analysis Date = 10/20/14 Pct Recovery = 68% Analysis Date = 10/15/14 Pct Recovery = 68% Analysis Date = 10/15/14 Pct Recovery = 68% Analysis Date = 10/10/14 Pct Recovery = 68% Analysis Date = 10/10/14 Pct Recovery = 68% Analysis Date = 10/05/14 Pct Recovery = 68% Analysis Date = 10/05/14 Pct Recovery = 68% Analysis Date = 09/30/14 Pct Recovery = 68% Analysis Date = 09/30/14 Pct Recovery = 68% Analysis Date = 09/25/14 Pct Recovery = 68% Analysis Date = 09/25/14 Pct Recovery = 68% Analysis Date = 09/20/14 Pct Recovery = 68% Analysis Date = 09/20/14 Pct Recovery = 68% Analysis Date = 09/15/14 Pct Recovery = 68% Analysis Date = 09/15/14 Pct Recovery = 68% Analysis Date = 09/10/14 Pct Recovery = 68% Analysis Date = 09/10/14 Pct Recovery = 68% Analysis Date = 09/05/14 Pct Recovery = 69% Analysis Date = 09/05/14 Pct Recovery = 69% Analysis Date = 08/31/14 Pct Recovery = 69% Analysis Date = 08/31/14 Pct Recovery = 69% Analysis Date = 08/26/14 Pct Recovery = 69% Analysis Date = 08/26/14 Pct Recovery = 69% Analysis Date = 08/21/14 Pct Recovery = 69% Analysis Date = 08/21/14 Pct Recovery = 69% Analysis Date = 08/16/14 Pct Recovery = 69% Analysis Date = 08/16/14 Pct Recovery = 69% Analysis Date = 08/11/14 Pct Recovery = 69% Analysis Date = 08/11/14 Pct Recovery = 69% Analysis Date = 08/06/14 Pct Recovery = 69% Analysis Date = 08/06/14 Pct Recovery = 69% Analysis Date = 08/01/14 Pct Recovery = 69% Analysis Date = 08/01/14 Pct Recovery = 69% Analysis Date = 07/27/14 Pct Recovery = 69% Analysis Date = 07/27/14 Pct Recovery = 69% Analysis Date = 07/22/14 Pct Recovery = 69% Analysis Date = 07/22/14 Pct Recovery = 69% Analysis Date = 07/17/14 Pct Recovery = 69% Analysis Date = 07/17/14 Pct Recovery = 69% Analysis Date = 07/12/14 Pct Recovery = 69% Analysis Date = 07/12/14 Pct Recovery = 69% Analysis Date = 07/07/14 Pct Recovery = 69% Analysis Date = 07/07/14 Pct Recovery = 69% Analysis Date = 07/02/14 Pct Recovery = 69% Analysis Date = 07/02/14 Pct Recovery = 69% Analysis Date = 06/27/14 Pct Recovery = 69% Analysis Date = 06/27/14 Pct Recovery = 69% Analysis Date = 06/22/14 Pct Recovery = 69% Analysis Date = 06/22/14 Pct Recovery = 69% Analysis Date = 06/17/14 Pct Recovery = 69% Analysis Date = 06/17/14 Pct Recovery = 69% Analysis Date = 06/12/14 Pct Recovery = 69% Analysis Date = 06/12/14 Pct Recovery = 69% Analysis Date = 06/07/14 Pct Recovery = 69% Analysis Date = 06/07/14 Pct Recovery = 69% Analysis Date = 06/02/14 Pct Recovery = 69% Analysis Date = 06/02/14 Pct Recovery = 69% Analysis Date = 05/28/14 Pct Recovery = 69% Analysis Date = 05/28/14 Pct Recovery = 69% Analysis Date = 05/23/14 Pct Recovery = 69% Analysis Date = 05/23/14 Pct Recovery = 69% Analysis Date = 05/18/14 Pct Recovery = 69% Analysis Date = 05/18/14 Pct Recovery = 69% Analysis Date = 05/13/14 Pct Recovery = 69% Analysis Date = 05/13/14 Pct Recovery = 69% Analysis Date = 05/08/14 Pct Recovery = 69% Analysis Date = 05/08/14 Pct Recovery = 69% Analysis Date = 05/03/14 Pct Recovery = 69% Analysis Date = 05/03/14 Pct Recovery = 69% Analysis Date = 04/28/14 Pct Recovery = 69% Analysis Date = 04/28/14 Pct Recovery = 69% Analysis Date = 04/23/14 Pct Recovery = 69% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
METAXALONE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 66 62% 23% 68% 17%
Total 66 62% 23% 68% 17%

Sample Statistics
METAXALONE

Characteristic N % % Basis
Plotted 66 85% Spiked
Estimated Values 59 76% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 2 3% Spiked
Spiked 78 .  
False Negatives 10 13% 10 out of 78
Not Spiked 37 .  
False Positives 0 0% 0 out of 37

BQS OBSP Determination:
METFORMIN
METHOD: 2440 , TESTIDCODE: 67492LCM56
Open Data Set

Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 78% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 74% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 78% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 74% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 80 µl & ERA 0406-15-08: 80 µl Pct Recovery = 42% Analysis Date = 11/04/15 SpikeMix = Abs 052215: 80 µl & Abs 050115: 80 µl Pct Recovery = 48% Analysis Date = 01/17/16 SpikeMix = ERA 0406-15-09: 80 µl & ERA 0406-15-07A: 80 µl Pct Recovery = 78% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 80 µl & Abs 051315: 80 µl Pct Recovery = 59% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 65% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 66% Analysis Date = 09/24/16 SpikeMix = Crescent EN160610015: 80 µl & Abs 061416: 80 µl Pct Recovery = 85% Analysis Date = 09/24/16 SpikeMix = Abs 061416: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 83% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 66% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 73% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 77% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 75% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-04: 15 µl & Abs 041814: 15 µl Pct Recovery = 70% Analysis Date = 02/06/15 SpikeMix = Abs 041814: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 73% Analysis Date = 07/12/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 55% Analysis Date = 06/22/14 SpikeMix = Abs 041814: 60 µl & Abs 041614: 60 µl Pct Recovery = 85% Analysis Date = 05/21/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 90% Analysis Date = 05/07/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 51% Analysis Date = 04/29/15 SpikeMix = ERA 0319-14-05: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 55% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 57% Analysis Date = 01/16/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 69% Analysis Date = 12/07/14 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 61% Analysis Date = 12/06/14 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 54% Analysis Date = 08/28/14 SpikeMix = ERA 0319-14-04: 60 µl & ERA 0319-14-05: 60 µl Pct Recovery = 43% Analysis Date = 07/26/14 SpikeMix = ERA 0319-14-05: 60 µl & ERA 0318-14-02: 60 µl Pct Recovery = 65% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 43% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 38% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 31% Analysis Date = 02/23/16 SpikeMix = Abs 052215: 40 µl & Abs 050115: 40 µl Pct Recovery = 40% Analysis Date = 07/31/15 SpikeMix = ERA 0406-15-09: 40 µl & Abs 050115: 40 µl Pct Recovery = 36% Analysis Date = 07/30/15 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 41% Analysis Date = 11/04/15 SpikeMix = ERA 0406-15-07A: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 59% Analysis Date = 09/10/15 SpikeMix = Abs 052215: 40 µl & ERA 0406-15-07A: 40 µl Pct Recovery = 72% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 62% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 68% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 75% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 82% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 56% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 59% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 73% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 63% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 60% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 66% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 73% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 77% Analysis Date = 04/10/15 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 68% Analysis Date = 11/04/14 SpikeMix = Abs 041814: 8 µl & ERA 0318-14-02: 8 µl Pct Recovery = 75% Analysis Date = 10/11/14 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 52% Analysis Date = 11/04/14 SpikeMix = Abs 041714: 8 µl & ERA 0319-14-05: 8 µl Pct Recovery = 50% Analysis Date = 10/24/14 SpikeMix = ERA 0319-14-05: 8 µl & Abs 041614: 8 µl Pct Recovery = 54% Analysis Date = 10/10/14 SpikeMix = Abs 041714: 30 µl & Abs 041814: 30 µl Pct Recovery = 70% Analysis Date = 10/10/14 SpikeMix = Abs 041814: 30 µl & ERA 0318-14-02: 30 µl Pct Recovery = 70% Analysis Date = 07/13/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 51% Analysis Date = 05/30/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 96% Analysis Date = 08/30/14 SpikeMix = ERA 0318-14-02: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 59% Analysis Date = 08/16/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 33% Analysis Date = 07/13/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 46% Analysis Date = 04/23/14 SpikeMix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.2: 20 µl Pct Recovery = 78% Analysis Date = 11/25/15 SpikeMix = Abs 050115: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 68% Analysis Date = 11/24/15 SpikeMix = ERA 0406-15-09: 20 µl & Abs 050115: 20 µl Pct Recovery = 53% Analysis Date = 08/27/15 SpikeMix = Abs 052215: 20 µl & Abs 050115: 20 µl Pct Recovery = 40% Analysis Date = 08/11/15 SpikeMix = Abs 050115: 20 µl & Abs 051315: 20 µl Pct Recovery = 39% Analysis Date = 07/09/15 SpikeMix = Abs 050115: 20 µl & Abs 052215: 20 µl Pct Recovery = 26% Analysis Date = 06/09/15 SpikeMix = Abs 051315: 20 µl & Abs 050115: 20 µl Pct Recovery = 43% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 52% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 48% Analysis Date = 04/27/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 84% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 13% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 22% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 55% Analysis Date = 11/24/15 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 93% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-09: 20 µl Pct Recovery = 54% Analysis Date = 01/18/17 Pct Recovery = 78% Analysis Date = 01/13/17 Pct Recovery = 77% Analysis Date = 01/13/17 Pct Recovery = 77% Analysis Date = 01/08/17 Pct Recovery = 77% Analysis Date = 01/08/17 Pct Recovery = 77% Analysis Date = 01/03/17 Pct Recovery = 77% Analysis Date = 01/03/17 Pct Recovery = 77% Analysis Date = 12/29/16 Pct Recovery = 76% Analysis Date = 12/29/16 Pct Recovery = 76% Analysis Date = 12/24/16 Pct Recovery = 76% Analysis Date = 12/24/16 Pct Recovery = 76% Analysis Date = 12/19/16 Pct Recovery = 75% Analysis Date = 12/19/16 Pct Recovery = 75% Analysis Date = 12/14/16 Pct Recovery = 75% Analysis Date = 12/14/16 Pct Recovery = 75% Analysis Date = 12/09/16 Pct Recovery = 74% Analysis Date = 12/09/16 Pct Recovery = 74% Analysis Date = 12/04/16 Pct Recovery = 74% Analysis Date = 12/04/16 Pct Recovery = 74% Analysis Date = 11/29/16 Pct Recovery = 74% Analysis Date = 11/29/16 Pct Recovery = 74% Analysis Date = 11/24/16 Pct Recovery = 73% Analysis Date = 11/24/16 Pct Recovery = 73% Analysis Date = 11/19/16 Pct Recovery = 73% Analysis Date = 11/19/16 Pct Recovery = 73% Analysis Date = 11/14/16 Pct Recovery = 72% Analysis Date = 11/14/16 Pct Recovery = 72% Analysis Date = 11/09/16 Pct Recovery = 72% Analysis Date = 11/09/16 Pct Recovery = 72% Analysis Date = 11/04/16 Pct Recovery = 71% Analysis Date = 11/04/16 Pct Recovery = 71% Analysis Date = 10/30/16 Pct Recovery = 71% Analysis Date = 10/30/16 Pct Recovery = 71% Analysis Date = 10/25/16 Pct Recovery = 71% Analysis Date = 10/25/16 Pct Recovery = 71% Analysis Date = 10/20/16 Pct Recovery = 70% Analysis Date = 10/20/16 Pct Recovery = 70% Analysis Date = 10/15/16 Pct Recovery = 70% Analysis Date = 10/15/16 Pct Recovery = 70% Analysis Date = 10/10/16 Pct Recovery = 69% Analysis Date = 10/10/16 Pct Recovery = 69% Analysis Date = 10/05/16 Pct Recovery = 69% Analysis Date = 10/05/16 Pct Recovery = 69% Analysis Date = 09/30/16 Pct Recovery = 68% Analysis Date = 09/30/16 Pct Recovery = 68% Analysis Date = 09/25/16 Pct Recovery = 68% Analysis Date = 09/25/16 Pct Recovery = 68% Analysis Date = 09/20/16 Pct Recovery = 67% Analysis Date = 09/20/16 Pct Recovery = 67% Analysis Date = 09/15/16 Pct Recovery = 67% Analysis Date = 09/15/16 Pct Recovery = 67% Analysis Date = 09/10/16 Pct Recovery = 67% Analysis Date = 09/10/16 Pct Recovery = 67% Analysis Date = 09/05/16 Pct Recovery = 66% Analysis Date = 09/05/16 Pct Recovery = 66% Analysis Date = 08/31/16 Pct Recovery = 66% Analysis Date = 08/31/16 Pct Recovery = 66% Analysis Date = 08/26/16 Pct Recovery = 65% Analysis Date = 08/26/16 Pct Recovery = 65% Analysis Date = 08/21/16 Pct Recovery = 65% Analysis Date = 08/21/16 Pct Recovery = 65% Analysis Date = 08/16/16 Pct Recovery = 65% Analysis Date = 08/16/16 Pct Recovery = 65% Analysis Date = 08/11/16 Pct Recovery = 64% Analysis Date = 08/11/16 Pct Recovery = 64% Analysis Date = 08/06/16 Pct Recovery = 64% Analysis Date = 08/06/16 Pct Recovery = 64% Analysis Date = 08/01/16 Pct Recovery = 63% Analysis Date = 08/01/16 Pct Recovery = 63% Analysis Date = 07/27/16 Pct Recovery = 63% Analysis Date = 07/27/16 Pct Recovery = 63% Analysis Date = 07/22/16 Pct Recovery = 63% Analysis Date = 07/22/16 Pct Recovery = 63% Analysis Date = 07/17/16 Pct Recovery = 62% Analysis Date = 07/17/16 Pct Recovery = 62% Analysis Date = 07/12/16 Pct Recovery = 62% Analysis Date = 07/12/16 Pct Recovery = 62% Analysis Date = 07/07/16 Pct Recovery = 62% Analysis Date = 07/07/16 Pct Recovery = 62% Analysis Date = 07/02/16 Pct Recovery = 61% Analysis Date = 07/02/16 Pct Recovery = 61% Analysis Date = 06/27/16 Pct Recovery = 61% Analysis Date = 06/27/16 Pct Recovery = 61% Analysis Date = 06/22/16 Pct Recovery = 61% Analysis Date = 06/22/16 Pct Recovery = 61% Analysis Date = 06/17/16 Pct Recovery = 60% Analysis Date = 06/17/16 Pct Recovery = 60% Analysis Date = 06/12/16 Pct Recovery = 60% Analysis Date = 06/12/16 Pct Recovery = 60% Analysis Date = 06/07/16 Pct Recovery = 60% Analysis Date = 06/07/16 Pct Recovery = 60% Analysis Date = 06/02/16 Pct Recovery = 59% Analysis Date = 06/02/16 Pct Recovery = 59% Analysis Date = 05/28/16 Pct Recovery = 59% Analysis Date = 05/28/16 Pct Recovery = 59% Analysis Date = 05/23/16 Pct Recovery = 59% Analysis Date = 05/23/16 Pct Recovery = 59% Analysis Date = 05/18/16 Pct Recovery = 58% Analysis Date = 05/18/16 Pct Recovery = 58% Analysis Date = 05/13/16 Pct Recovery = 58% Analysis Date = 05/13/16 Pct Recovery = 58% Analysis Date = 05/08/16 Pct Recovery = 58% Analysis Date = 05/08/16 Pct Recovery = 58% Analysis Date = 05/03/16 Pct Recovery = 57% Analysis Date = 05/03/16 Pct Recovery = 57% Analysis Date = 04/28/16 Pct Recovery = 57% Analysis Date = 04/28/16 Pct Recovery = 57% Analysis Date = 04/23/16 Pct Recovery = 57% Analysis Date = 04/23/16 Pct Recovery = 57% Analysis Date = 04/18/16 Pct Recovery = 57% Analysis Date = 04/18/16 Pct Recovery = 57% Analysis Date = 04/13/16 Pct Recovery = 56% Analysis Date = 04/13/16 Pct Recovery = 56% Analysis Date = 04/08/16 Pct Recovery = 56% Analysis Date = 04/08/16 Pct Recovery = 56% Analysis Date = 04/03/16 Pct Recovery = 56% Analysis Date = 04/03/16 Pct Recovery = 56% Analysis Date = 03/29/16 Pct Recovery = 56% Analysis Date = 03/29/16 Pct Recovery = 56% Analysis Date = 03/24/16 Pct Recovery = 56% Analysis Date = 03/24/16 Pct Recovery = 56% Analysis Date = 03/19/16 Pct Recovery = 55% Analysis Date = 03/19/16 Pct Recovery = 55% Analysis Date = 03/14/16 Pct Recovery = 55% Analysis Date = 03/14/16 Pct Recovery = 55% Analysis Date = 03/09/16 Pct Recovery = 55% Analysis Date = 03/09/16 Pct Recovery = 55% Analysis Date = 03/04/16 Pct Recovery = 55% Analysis Date = 03/04/16 Pct Recovery = 55% Analysis Date = 02/28/16 Pct Recovery = 55% Analysis Date = 02/28/16 Pct Recovery = 55% Analysis Date = 02/23/16 Pct Recovery = 54% Analysis Date = 02/23/16 Pct Recovery = 54% Analysis Date = 02/18/16 Pct Recovery = 54% Analysis Date = 02/18/16 Pct Recovery = 54% Analysis Date = 02/13/16 Pct Recovery = 54% Analysis Date = 02/13/16 Pct Recovery = 54% Analysis Date = 02/08/16 Pct Recovery = 54% Analysis Date = 02/08/16 Pct Recovery = 54% Analysis Date = 02/03/16 Pct Recovery = 54% Analysis Date = 02/03/16 Pct Recovery = 54% Analysis Date = 01/29/16 Pct Recovery = 53% Analysis Date = 01/29/16 Pct Recovery = 53% Analysis Date = 01/24/16 Pct Recovery = 53% Analysis Date = 01/24/16 Pct Recovery = 53% Analysis Date = 01/19/16 Pct Recovery = 53% Analysis Date = 01/19/16 Pct Recovery = 53% Analysis Date = 01/14/16 Pct Recovery = 53% Analysis Date = 01/14/16 Pct Recovery = 53% Analysis Date = 01/09/16 Pct Recovery = 53% Analysis Date = 01/09/16 Pct Recovery = 53% Analysis Date = 01/04/16 Pct Recovery = 52% Analysis Date = 01/04/16 Pct Recovery = 52% Analysis Date = 12/30/15 Pct Recovery = 52% Analysis Date = 12/30/15 Pct Recovery = 52% Analysis Date = 12/25/15 Pct Recovery = 52% Analysis Date = 12/25/15 Pct Recovery = 52% Analysis Date = 12/20/15 Pct Recovery = 52% Analysis Date = 12/20/15 Pct Recovery = 52% Analysis Date = 12/15/15 Pct Recovery = 52% Analysis Date = 12/15/15 Pct Recovery = 52% Analysis Date = 12/10/15 Pct Recovery = 52% Analysis Date = 12/10/15 Pct Recovery = 52% Analysis Date = 12/05/15 Pct Recovery = 51% Analysis Date = 12/05/15 Pct Recovery = 51% Analysis Date = 11/30/15 Pct Recovery = 51% Analysis Date = 11/30/15 Pct Recovery = 51% Analysis Date = 11/25/15 Pct Recovery = 51% Analysis Date = 11/25/15 Pct Recovery = 51% Analysis Date = 11/20/15 Pct Recovery = 51% Analysis Date = 11/20/15 Pct Recovery = 51% Analysis Date = 11/15/15 Pct Recovery = 51% Analysis Date = 11/15/15 Pct Recovery = 51% Analysis Date = 11/10/15 Pct Recovery = 51% Analysis Date = 11/10/15 Pct Recovery = 51% Analysis Date = 11/05/15 Pct Recovery = 51% Analysis Date = 11/05/15 Pct Recovery = 51% Analysis Date = 10/31/15 Pct Recovery = 52% Analysis Date = 10/31/15 Pct Recovery = 52% Analysis Date = 10/26/15 Pct Recovery = 52% Analysis Date = 10/26/15 Pct Recovery = 52% Analysis Date = 10/21/15 Pct Recovery = 52% Analysis Date = 10/21/15 Pct Recovery = 52% Analysis Date = 10/16/15 Pct Recovery = 52% Analysis Date = 10/16/15 Pct Recovery = 52% Analysis Date = 10/11/15 Pct Recovery = 52% Analysis Date = 10/11/15 Pct Recovery = 52% Analysis Date = 10/06/15 Pct Recovery = 52% Analysis Date = 10/06/15 Pct Recovery = 52% Analysis Date = 10/01/15 Pct Recovery = 52% Analysis Date = 10/01/15 Pct Recovery = 52% Analysis Date = 09/26/15 Pct Recovery = 53% Analysis Date = 09/26/15 Pct Recovery = 53% Analysis Date = 09/21/15 Pct Recovery = 53% Analysis Date = 09/21/15 Pct Recovery = 53% Analysis Date = 09/16/15 Pct Recovery = 53% Analysis Date = 09/16/15 Pct Recovery = 53% Analysis Date = 09/11/15 Pct Recovery = 53% Analysis Date = 09/11/15 Pct Recovery = 53% Analysis Date = 09/05/15 Pct Recovery = 53% Analysis Date = 09/05/15 Pct Recovery = 53% Analysis Date = 08/31/15 Pct Recovery = 53% Analysis Date = 08/31/15 Pct Recovery = 53% Analysis Date = 08/26/15 Pct Recovery = 53% Analysis Date = 08/26/15 Pct Recovery = 53% Analysis Date = 08/21/15 Pct Recovery = 54% Analysis Date = 08/21/15 Pct Recovery = 54% Analysis Date = 08/16/15 Pct Recovery = 54% Analysis Date = 08/16/15 Pct Recovery = 54% Analysis Date = 08/11/15 Pct Recovery = 54% Analysis Date = 08/11/15 Pct Recovery = 54% Analysis Date = 08/06/15 Pct Recovery = 54% Analysis Date = 08/06/15 Pct Recovery = 54% Analysis Date = 08/01/15 Pct Recovery = 54% Analysis Date = 08/01/15 Pct Recovery = 54% Analysis Date = 07/27/15 Pct Recovery = 54% Analysis Date = 07/27/15 Pct Recovery = 54% Analysis Date = 07/22/15 Pct Recovery = 54% Analysis Date = 07/22/15 Pct Recovery = 54% Analysis Date = 07/17/15 Pct Recovery = 54% Analysis Date = 07/17/15 Pct Recovery = 54% Analysis Date = 07/12/15 Pct Recovery = 55% Analysis Date = 07/12/15 Pct Recovery = 55% Analysis Date = 07/07/15 Pct Recovery = 55% Analysis Date = 07/07/15 Pct Recovery = 55% Analysis Date = 07/02/15 Pct Recovery = 55% Analysis Date = 07/02/15 Pct Recovery = 55% Analysis Date = 06/27/15 Pct Recovery = 55% Analysis Date = 06/27/15 Pct Recovery = 55% Analysis Date = 06/22/15 Pct Recovery = 55% Analysis Date = 06/22/15 Pct Recovery = 55% Analysis Date = 06/17/15 Pct Recovery = 55% Analysis Date = 06/17/15 Pct Recovery = 55% Analysis Date = 06/12/15 Pct Recovery = 55% Analysis Date = 06/12/15 Pct Recovery = 55% Analysis Date = 06/07/15 Pct Recovery = 55% Analysis Date = 06/07/15 Pct Recovery = 55% Analysis Date = 06/02/15 Pct Recovery = 55% Analysis Date = 06/02/15 Pct Recovery = 55% Analysis Date = 05/28/15 Pct Recovery = 55% Analysis Date = 05/28/15 Pct Recovery = 55% Analysis Date = 05/23/15 Pct Recovery = 55% Analysis Date = 05/23/15 Pct Recovery = 55% Analysis Date = 05/18/15 Pct Recovery = 55% Analysis Date = 05/18/15 Pct Recovery = 55% Analysis Date = 05/13/15 Pct Recovery = 55% Analysis Date = 05/13/15 Pct Recovery = 55% Analysis Date = 05/08/15 Pct Recovery = 55% Analysis Date = 05/08/15 Pct Recovery = 55% Analysis Date = 05/03/15 Pct Recovery = 55% Analysis Date = 05/03/15 Pct Recovery = 55% Analysis Date = 04/28/15 Pct Recovery = 55% Analysis Date = 04/28/15 Pct Recovery = 55% Analysis Date = 04/23/15 Pct Recovery = 56% Analysis Date = 04/23/15 Pct Recovery = 56% Analysis Date = 04/18/15 Pct Recovery = 56% Analysis Date = 04/18/15 Pct Recovery = 56% Analysis Date = 04/13/15 Pct Recovery = 56% Analysis Date = 04/13/15 Pct Recovery = 56% Analysis Date = 04/08/15 Pct Recovery = 56% Analysis Date = 04/08/15 Pct Recovery = 56% Analysis Date = 04/03/15 Pct Recovery = 56% Analysis Date = 04/03/15 Pct Recovery = 56% Analysis Date = 03/29/15 Pct Recovery = 56% Analysis Date = 03/29/15 Pct Recovery = 56% Analysis Date = 03/24/15 Pct Recovery = 56% Analysis Date = 03/24/15 Pct Recovery = 56% Analysis Date = 03/19/15 Pct Recovery = 56% Analysis Date = 03/19/15 Pct Recovery = 56% Analysis Date = 03/14/15 Pct Recovery = 57% Analysis Date = 03/14/15 Pct Recovery = 57% Analysis Date = 03/09/15 Pct Recovery = 57% Analysis Date = 03/09/15 Pct Recovery = 57% Analysis Date = 03/04/15 Pct Recovery = 57% Analysis Date = 03/04/15 Pct Recovery = 57% Analysis Date = 02/27/15 Pct Recovery = 57% Analysis Date = 02/27/15 Pct Recovery = 57% Analysis Date = 02/22/15 Pct Recovery = 57% Analysis Date = 02/22/15 Pct Recovery = 57% Analysis Date = 02/17/15 Pct Recovery = 57% Analysis Date = 02/17/15 Pct Recovery = 57% Analysis Date = 02/12/15 Pct Recovery = 57% Analysis Date = 02/12/15 Pct Recovery = 57% Analysis Date = 02/07/15 Pct Recovery = 58% Analysis Date = 02/07/15 Pct Recovery = 58% Analysis Date = 02/02/15 Pct Recovery = 58% Analysis Date = 02/02/15 Pct Recovery = 58% Analysis Date = 01/28/15 Pct Recovery = 58% Analysis Date = 01/28/15 Pct Recovery = 58% Analysis Date = 01/23/15 Pct Recovery = 58% Analysis Date = 01/23/15 Pct Recovery = 58% Analysis Date = 01/18/15 Pct Recovery = 58% Analysis Date = 01/18/15 Pct Recovery = 58% Analysis Date = 01/13/15 Pct Recovery = 58% Analysis Date = 01/13/15 Pct Recovery = 58% Analysis Date = 01/08/15 Pct Recovery = 58% Analysis Date = 01/08/15 Pct Recovery = 58% Analysis Date = 01/03/15 Pct Recovery = 59% Analysis Date = 01/03/15 Pct Recovery = 59% Analysis Date = 12/29/14 Pct Recovery = 59% Analysis Date = 12/29/14 Pct Recovery = 59% Analysis Date = 12/24/14 Pct Recovery = 59% Analysis Date = 12/24/14 Pct Recovery = 59% Analysis Date = 12/19/14 Pct Recovery = 59% Analysis Date = 12/19/14 Pct Recovery = 59% Analysis Date = 12/14/14 Pct Recovery = 59% Analysis Date = 12/14/14 Pct Recovery = 59% Analysis Date = 12/09/14 Pct Recovery = 59% Analysis Date = 12/09/14 Pct Recovery = 59% Analysis Date = 12/04/14 Pct Recovery = 60% Analysis Date = 12/04/14 Pct Recovery = 60% Analysis Date = 11/29/14 Pct Recovery = 60% Analysis Date = 11/29/14 Pct Recovery = 60% Analysis Date = 11/24/14 Pct Recovery = 60% Analysis Date = 11/24/14 Pct Recovery = 60% Analysis Date = 11/19/14 Pct Recovery = 60% Analysis Date = 11/19/14 Pct Recovery = 60% Analysis Date = 11/14/14 Pct Recovery = 60% Analysis Date = 11/14/14 Pct Recovery = 60% Analysis Date = 11/09/14 Pct Recovery = 61% Analysis Date = 11/09/14 Pct Recovery = 61% Analysis Date = 11/04/14 Pct Recovery = 61% Analysis Date = 11/04/14 Pct Recovery = 61% Analysis Date = 10/30/14 Pct Recovery = 61% Analysis Date = 10/30/14 Pct Recovery = 61% Analysis Date = 10/25/14 Pct Recovery = 61% Analysis Date = 10/25/14 Pct Recovery = 61% Analysis Date = 10/20/14 Pct Recovery = 61% Analysis Date = 10/20/14 Pct Recovery = 61% Analysis Date = 10/15/14 Pct Recovery = 62% Analysis Date = 10/15/14 Pct Recovery = 62% Analysis Date = 10/10/14 Pct Recovery = 62% Analysis Date = 10/10/14 Pct Recovery = 62% Analysis Date = 10/05/14 Pct Recovery = 62% Analysis Date = 10/05/14 Pct Recovery = 62% Analysis Date = 09/30/14 Pct Recovery = 62% Analysis Date = 09/30/14 Pct Recovery = 62% Analysis Date = 09/25/14 Pct Recovery = 63% Analysis Date = 09/25/14 Pct Recovery = 63% Analysis Date = 09/20/14 Pct Recovery = 63% Analysis Date = 09/20/14 Pct Recovery = 63% Analysis Date = 09/15/14 Pct Recovery = 63% Analysis Date = 09/15/14 Pct Recovery = 63% Analysis Date = 09/10/14 Pct Recovery = 63% Analysis Date = 09/10/14 Pct Recovery = 63% Analysis Date = 09/05/14 Pct Recovery = 63% Analysis Date = 09/05/14 Pct Recovery = 63% Analysis Date = 08/31/14 Pct Recovery = 64% Analysis Date = 08/31/14 Pct Recovery = 64% Analysis Date = 08/26/14 Pct Recovery = 64% Analysis Date = 08/26/14 Pct Recovery = 64% Analysis Date = 08/21/14 Pct Recovery = 64% Analysis Date = 08/21/14 Pct Recovery = 64% Analysis Date = 08/16/14 Pct Recovery = 64% Analysis Date = 08/16/14 Pct Recovery = 64% Analysis Date = 08/11/14 Pct Recovery = 64% Analysis Date = 08/11/14 Pct Recovery = 64% Analysis Date = 08/06/14 Pct Recovery = 65% Analysis Date = 08/06/14 Pct Recovery = 65% Analysis Date = 08/01/14 Pct Recovery = 65% Analysis Date = 08/01/14 Pct Recovery = 65% Analysis Date = 07/27/14 Pct Recovery = 65% Analysis Date = 07/27/14 Pct Recovery = 65% Analysis Date = 07/22/14 Pct Recovery = 65% Analysis Date = 07/22/14 Pct Recovery = 65% Analysis Date = 07/17/14 Pct Recovery = 66% Analysis Date = 07/17/14 Pct Recovery = 66% Analysis Date = 07/12/14 Pct Recovery = 66% Analysis Date = 07/12/14 Pct Recovery = 66% Analysis Date = 07/07/14 Pct Recovery = 66% Analysis Date = 07/07/14 Pct Recovery = 66% Analysis Date = 07/02/14 Pct Recovery = 66% Analysis Date = 07/02/14 Pct Recovery = 66% Analysis Date = 06/27/14 Pct Recovery = 66% Analysis Date = 06/27/14 Pct Recovery = 66% Analysis Date = 06/22/14 Pct Recovery = 67% Analysis Date = 06/22/14 Pct Recovery = 67% Analysis Date = 06/17/14 Pct Recovery = 67% Analysis Date = 06/17/14 Pct Recovery = 67% Analysis Date = 06/12/14 Pct Recovery = 67% Analysis Date = 06/12/14 Pct Recovery = 67% Analysis Date = 06/07/14 Pct Recovery = 67% Analysis Date = 06/07/14 Pct Recovery = 67% Analysis Date = 06/02/14 Pct Recovery = 67% Analysis Date = 06/02/14 Pct Recovery = 67% Analysis Date = 05/28/14 Pct Recovery = 68% Analysis Date = 05/28/14 Pct Recovery = 68% Analysis Date = 05/23/14 Pct Recovery = 68% Analysis Date = 05/23/14 Pct Recovery = 68% Analysis Date = 05/18/14 Pct Recovery = 68% Analysis Date = 05/18/14 Pct Recovery = 68% Analysis Date = 05/13/14 Pct Recovery = 68% Analysis Date = 05/13/14 Pct Recovery = 68% Analysis Date = 05/08/14 Pct Recovery = 69% Analysis Date = 05/08/14 Pct Recovery = 69% Analysis Date = 05/03/14 Pct Recovery = 69% Analysis Date = 05/03/14 Pct Recovery = 69% Analysis Date = 04/28/14 Pct Recovery = 69% Analysis Date = 04/28/14 Pct Recovery = 69% Analysis Date = 04/23/14 Pct Recovery = 69% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
METFORMIN

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 76 61% 17% 61% 17%
Total 76 61% 17% 61% 17%

Sample Statistics
METFORMIN

Characteristic N % % Basis
Plotted 76 97% Spiked
Estimated Values 8 10% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 78 .  
False Negatives 2 3% 2 out of 78
Not Spiked 37 .  
False Positives 1 3% 1 out of 37

BQS OBSP Determination:
METHADONE
METHOD: 2440 , TESTIDCODE: 67500LCM56
Open Data Set

Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 85% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 84% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 88% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 104% Analysis Date = 11/24/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 71% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 72% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 73% Analysis Date = 09/24/16 SpikeMix = Crescent EN160610015: 80 µl & Abs 061416: 80 µl Pct Recovery = 59% Analysis Date = 09/24/16 SpikeMix = Abs 061416: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 61% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 67% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 74% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 72% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 75% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 65% Analysis Date = 12/07/14 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 61% Analysis Date = 10/25/14 SpikeMix = Abs 041614: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 68% Analysis Date = 06/22/14 SpikeMix = Abs 041814: 60 µl & Abs 041614: 60 µl Pct Recovery = 80% Analysis Date = 06/11/14 SpikeMix = Abs 041614: 60 µl & Abs 041714: 60 µl Pct Recovery = 63% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 63% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 53% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-07A: 40 µl & Abs 051315: 40 µl Pct Recovery = 53% Analysis Date = 07/31/15 SpikeMix = Abs 051315: 40 µl & Abs 052215: 40 µl Pct Recovery = 106% Analysis Date = 07/30/15 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 117% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 94% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 80% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 69% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 64% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 69% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 73% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 61% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 59% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 67% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 57% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 61% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 61% Analysis Date = 04/30/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 55% Analysis Date = 02/10/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 41% Analysis Date = 10/24/14 SpikeMix = ERA 0319-14-05: 8 µl & Abs 041614: 8 µl Pct Recovery = 59% Analysis Date = 09/12/14 SpikeMix = Abs 041614: 30 µl & ERA 0319-14-04: 30 µl Pct Recovery = 42% Analysis Date = 07/13/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 55% Analysis Date = 06/28/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 56% Analysis Date = 05/30/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 59% Analysis Date = 05/17/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 62% Analysis Date = 02/23/16 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 49% Analysis Date = 08/11/15 SpikeMix = Abs 050115: 20 µl & Abs 051315: 20 µl Pct Recovery = 71% Analysis Date = 06/26/15 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 55% Analysis Date = 06/09/15 SpikeMix = Abs 051315: 20 µl & Abs 050115: 20 µl Pct Recovery = 47% Analysis Date = 01/18/17 Pct Recovery = 89% Analysis Date = 01/14/17 Pct Recovery = 88% Analysis Date = 01/14/17 Pct Recovery = 88% Analysis Date = 01/09/17 Pct Recovery = 87% Analysis Date = 01/09/17 Pct Recovery = 87% Analysis Date = 01/04/17 Pct Recovery = 86% Analysis Date = 01/04/17 Pct Recovery = 86% Analysis Date = 12/30/16 Pct Recovery = 85% Analysis Date = 12/30/16 Pct Recovery = 85% Analysis Date = 12/25/16 Pct Recovery = 85% Analysis Date = 12/25/16 Pct Recovery = 85% Analysis Date = 12/20/16 Pct Recovery = 84% Analysis Date = 12/20/16 Pct Recovery = 84% Analysis Date = 12/15/16 Pct Recovery = 83% Analysis Date = 12/15/16 Pct Recovery = 83% Analysis Date = 12/10/16 Pct Recovery = 82% Analysis Date = 12/10/16 Pct Recovery = 82% Analysis Date = 12/05/16 Pct Recovery = 82% Analysis Date = 12/05/16 Pct Recovery = 82% Analysis Date = 12/01/16 Pct Recovery = 81% Analysis Date = 12/01/16 Pct Recovery = 81% Analysis Date = 11/26/16 Pct Recovery = 80% Analysis Date = 11/26/16 Pct Recovery = 80% Analysis Date = 11/21/16 Pct Recovery = 79% Analysis Date = 11/21/16 Pct Recovery = 79% Analysis Date = 11/16/16 Pct Recovery = 78% Analysis Date = 11/16/16 Pct Recovery = 78% Analysis Date = 11/11/16 Pct Recovery = 78% Analysis Date = 11/11/16 Pct Recovery = 78% Analysis Date = 11/06/16 Pct Recovery = 77% Analysis Date = 11/06/16 Pct Recovery = 77% Analysis Date = 11/01/16 Pct Recovery = 76% Analysis Date = 11/01/16 Pct Recovery = 76% Analysis Date = 10/27/16 Pct Recovery = 76% Analysis Date = 10/27/16 Pct Recovery = 76% Analysis Date = 10/22/16 Pct Recovery = 75% Analysis Date = 10/22/16 Pct Recovery = 75% Analysis Date = 10/18/16 Pct Recovery = 74% Analysis Date = 10/18/16 Pct Recovery = 74% Analysis Date = 10/13/16 Pct Recovery = 73% Analysis Date = 10/13/16 Pct Recovery = 73% Analysis Date = 10/08/16 Pct Recovery = 73% Analysis Date = 10/08/16 Pct Recovery = 73% Analysis Date = 10/03/16 Pct Recovery = 72% Analysis Date = 10/03/16 Pct Recovery = 72% Analysis Date = 09/28/16 Pct Recovery = 71% Analysis Date = 09/28/16 Pct Recovery = 71% Analysis Date = 09/23/16 Pct Recovery = 71% Analysis Date = 09/23/16 Pct Recovery = 71% Analysis Date = 09/18/16 Pct Recovery = 70% Analysis Date = 09/18/16 Pct Recovery = 70% Analysis Date = 09/13/16 Pct Recovery = 69% Analysis Date = 09/13/16 Pct Recovery = 69% Analysis Date = 09/08/16 Pct Recovery = 69% Analysis Date = 09/08/16 Pct Recovery = 69% Analysis Date = 09/04/16 Pct Recovery = 68% Analysis Date = 09/04/16 Pct Recovery = 68% Analysis Date = 08/30/16 Pct Recovery = 67% Analysis Date = 08/30/16 Pct Recovery = 67% Analysis Date = 08/25/16 Pct Recovery = 67% Analysis Date = 08/25/16 Pct Recovery = 67% Analysis Date = 08/20/16 Pct Recovery = 66% Analysis Date = 08/20/16 Pct Recovery = 66% Analysis Date = 08/15/16 Pct Recovery = 66% Analysis Date = 08/15/16 Pct Recovery = 66% Analysis Date = 08/10/16 Pct Recovery = 65% Analysis Date = 08/10/16 Pct Recovery = 65% Analysis Date = 08/05/16 Pct Recovery = 65% Analysis Date = 08/05/16 Pct Recovery = 65% Analysis Date = 07/31/16 Pct Recovery = 64% Analysis Date = 07/31/16 Pct Recovery = 64% Analysis Date = 07/26/16 Pct Recovery = 64% Analysis Date = 07/26/16 Pct Recovery = 64% Analysis Date = 07/22/16 Pct Recovery = 63% Analysis Date = 07/22/16 Pct Recovery = 63% Analysis Date = 07/17/16 Pct Recovery = 63% Analysis Date = 07/17/16 Pct Recovery = 63% Analysis Date = 07/12/16 Pct Recovery = 63% Analysis Date = 07/12/16 Pct Recovery = 63% Analysis Date = 07/07/16 Pct Recovery = 63% Analysis Date = 07/07/16 Pct Recovery = 63% Analysis Date = 07/02/16 Pct Recovery = 63% Analysis Date = 07/02/16 Pct Recovery = 63% Analysis Date = 06/27/16 Pct Recovery = 63% Analysis Date = 06/27/16 Pct Recovery = 63% Analysis Date = 06/22/16 Pct Recovery = 63% Analysis Date = 06/22/16 Pct Recovery = 63% Analysis Date = 06/17/16 Pct Recovery = 63% Analysis Date = 06/17/16 Pct Recovery = 63% Analysis Date = 06/12/16 Pct Recovery = 63% Analysis Date = 06/12/16 Pct Recovery = 63% Analysis Date = 06/08/16 Pct Recovery = 63% Analysis Date = 06/08/16 Pct Recovery = 63% Analysis Date = 06/03/16 Pct Recovery = 63% Analysis Date = 06/03/16 Pct Recovery = 63% Analysis Date = 05/29/16 Pct Recovery = 63% Analysis Date = 05/29/16 Pct Recovery = 63% Analysis Date = 05/24/16 Pct Recovery = 63% Analysis Date = 05/24/16 Pct Recovery = 63% Analysis Date = 05/19/16 Pct Recovery = 63% Analysis Date = 05/19/16 Pct Recovery = 63% Analysis Date = 05/14/16 Pct Recovery = 63% Analysis Date = 05/14/16 Pct Recovery = 63% Analysis Date = 05/09/16 Pct Recovery = 63% Analysis Date = 05/09/16 Pct Recovery = 63% Analysis Date = 05/04/16 Pct Recovery = 63% Analysis Date = 05/04/16 Pct Recovery = 63% Analysis Date = 04/29/16 Pct Recovery = 63% Analysis Date = 04/29/16 Pct Recovery = 63% Analysis Date = 04/25/16 Pct Recovery = 63% Analysis Date = 04/25/16 Pct Recovery = 63% Analysis Date = 04/20/16 Pct Recovery = 63% Analysis Date = 04/20/16 Pct Recovery = 63% Analysis Date = 04/15/16 Pct Recovery = 63% Analysis Date = 04/15/16 Pct Recovery = 63% Analysis Date = 04/10/16 Pct Recovery = 63% Analysis Date = 04/10/16 Pct Recovery = 63% Analysis Date = 04/05/16 Pct Recovery = 63% Analysis Date = 04/05/16 Pct Recovery = 63% Analysis Date = 03/31/16 Pct Recovery = 63% Analysis Date = 03/31/16 Pct Recovery = 63% Analysis Date = 03/26/16 Pct Recovery = 63% Analysis Date = 03/26/16 Pct Recovery = 63% Analysis Date = 03/21/16 Pct Recovery = 63% Analysis Date = 03/21/16 Pct Recovery = 63% Analysis Date = 03/16/16 Pct Recovery = 63% Analysis Date = 03/16/16 Pct Recovery = 63% Analysis Date = 03/12/16 Pct Recovery = 63% Analysis Date = 03/12/16 Pct Recovery = 63% Analysis Date = 03/07/16 Pct Recovery = 64% Analysis Date = 03/07/16 Pct Recovery = 64% Analysis Date = 03/02/16 Pct Recovery = 64% Analysis Date = 03/02/16 Pct Recovery = 64% Analysis Date = 02/26/16 Pct Recovery = 64% Analysis Date = 02/26/16 Pct Recovery = 64% Analysis Date = 02/21/16 Pct Recovery = 64% Analysis Date = 02/21/16 Pct Recovery = 64% Analysis Date = 02/16/16 Pct Recovery = 64% Analysis Date = 02/16/16 Pct Recovery = 64% Analysis Date = 02/11/16 Pct Recovery = 64% Analysis Date = 02/11/16 Pct Recovery = 64% Analysis Date = 02/06/16 Pct Recovery = 64% Analysis Date = 02/06/16 Pct Recovery = 64% Analysis Date = 02/01/16 Pct Recovery = 64% Analysis Date = 02/01/16 Pct Recovery = 64% Analysis Date = 01/28/16 Pct Recovery = 64% Analysis Date = 01/28/16 Pct Recovery = 64% Analysis Date = 01/23/16 Pct Recovery = 64% Analysis Date = 01/23/16 Pct Recovery = 64% Analysis Date = 01/18/16 Pct Recovery = 64% Analysis Date = 01/18/16 Pct Recovery = 64% Analysis Date = 01/13/16 Pct Recovery = 64% Analysis Date = 01/13/16 Pct Recovery = 64% Analysis Date = 01/08/16 Pct Recovery = 64% Analysis Date = 01/08/16 Pct Recovery = 64% Analysis Date = 01/03/16 Pct Recovery = 64% Analysis Date = 01/03/16 Pct Recovery = 64% Analysis Date = 12/29/15 Pct Recovery = 65% Analysis Date = 12/29/15 Pct Recovery = 65% Analysis Date = 12/24/15 Pct Recovery = 65% Analysis Date = 12/24/15 Pct Recovery = 65% Analysis Date = 12/19/15 Pct Recovery = 65% Analysis Date = 12/19/15 Pct Recovery = 65% Analysis Date = 12/15/15 Pct Recovery = 65% Analysis Date = 12/15/15 Pct Recovery = 65% Analysis Date = 12/10/15 Pct Recovery = 65% Analysis Date = 12/10/15 Pct Recovery = 65% Analysis Date = 12/05/15 Pct Recovery = 65% Analysis Date = 12/05/15 Pct Recovery = 65% Analysis Date = 11/30/15 Pct Recovery = 65% Analysis Date = 11/30/15 Pct Recovery = 65% Analysis Date = 11/25/15 Pct Recovery = 65% Analysis Date = 11/25/15 Pct Recovery = 65% Analysis Date = 11/20/15 Pct Recovery = 65% Analysis Date = 11/20/15 Pct Recovery = 65% Analysis Date = 11/15/15 Pct Recovery = 65% Analysis Date = 11/15/15 Pct Recovery = 65% Analysis Date = 11/10/15 Pct Recovery = 65% Analysis Date = 11/10/15 Pct Recovery = 65% Analysis Date = 11/05/15 Pct Recovery = 65% Analysis Date = 11/05/15 Pct Recovery = 65% Analysis Date = 11/01/15 Pct Recovery = 66% Analysis Date = 11/01/15 Pct Recovery = 66% Analysis Date = 10/27/15 Pct Recovery = 66% Analysis Date = 10/27/15 Pct Recovery = 66% Analysis Date = 10/22/15 Pct Recovery = 66% Analysis Date = 10/22/15 Pct Recovery = 66% Analysis Date = 10/17/15 Pct Recovery = 66% Analysis Date = 10/17/15 Pct Recovery = 66% Analysis Date = 10/12/15 Pct Recovery = 66% Analysis Date = 10/12/15 Pct Recovery = 66% Analysis Date = 10/07/15 Pct Recovery = 66% Analysis Date = 10/07/15 Pct Recovery = 66% Analysis Date = 10/02/15 Pct Recovery = 66% Analysis Date = 10/02/15 Pct Recovery = 66% Analysis Date = 09/27/15 Pct Recovery = 66% Analysis Date = 09/27/15 Pct Recovery = 66% Analysis Date = 09/22/15 Pct Recovery = 66% Analysis Date = 09/22/15 Pct Recovery = 66% Analysis Date = 09/17/15 Pct Recovery = 66% Analysis Date = 09/17/15 Pct Recovery = 66% Analysis Date = 09/13/15 Pct Recovery = 66% Analysis Date = 09/13/15 Pct Recovery = 66% Analysis Date = 09/08/15 Pct Recovery = 66% Analysis Date = 09/08/15 Pct Recovery = 66% Analysis Date = 09/03/15 Pct Recovery = 67% Analysis Date = 09/03/15 Pct Recovery = 67% Analysis Date = 08/29/15 Pct Recovery = 67% Analysis Date = 08/29/15 Pct Recovery = 67% Analysis Date = 08/24/15 Pct Recovery = 67% Analysis Date = 08/24/15 Pct Recovery = 67% Analysis Date = 08/19/15 Pct Recovery = 67% Analysis Date = 08/19/15 Pct Recovery = 67% Analysis Date = 08/14/15 Pct Recovery = 67% Analysis Date = 08/14/15 Pct Recovery = 67% Analysis Date = 08/09/15 Pct Recovery = 67% Analysis Date = 08/09/15 Pct Recovery = 67% Analysis Date = 08/04/15 Pct Recovery = 67% Analysis Date = 08/04/15 Pct Recovery = 67% Analysis Date = 07/31/15 Pct Recovery = 67% Analysis Date = 07/31/15 Pct Recovery = 67% Analysis Date = 07/26/15 Pct Recovery = 67% Analysis Date = 07/26/15 Pct Recovery = 67% Analysis Date = 07/21/15 Pct Recovery = 67% Analysis Date = 07/21/15 Pct Recovery = 67% Analysis Date = 07/16/15 Pct Recovery = 67% Analysis Date = 07/16/15 Pct Recovery = 67% Analysis Date = 07/11/15 Pct Recovery = 67% Analysis Date = 07/11/15 Pct Recovery = 67% Analysis Date = 07/06/15 Pct Recovery = 67% Analysis Date = 07/06/15 Pct Recovery = 67% Analysis Date = 07/01/15 Pct Recovery = 66% Analysis Date = 07/01/15 Pct Recovery = 66% Analysis Date = 06/26/15 Pct Recovery = 66% Analysis Date = 06/26/15 Pct Recovery = 66% Analysis Date = 06/21/15 Pct Recovery = 66% Analysis Date = 06/21/15 Pct Recovery = 66% Analysis Date = 06/17/15 Pct Recovery = 66% Analysis Date = 06/17/15 Pct Recovery = 66% Analysis Date = 06/12/15 Pct Recovery = 66% Analysis Date = 06/12/15 Pct Recovery = 66% Analysis Date = 06/07/15 Pct Recovery = 66% Analysis Date = 06/07/15 Pct Recovery = 66% Analysis Date = 06/02/15 Pct Recovery = 66% Analysis Date = 06/02/15 Pct Recovery = 66% Analysis Date = 05/28/15 Pct Recovery = 66% Analysis Date = 05/28/15 Pct Recovery = 66% Analysis Date = 05/23/15 Pct Recovery = 66% Analysis Date = 05/23/15 Pct Recovery = 66% Analysis Date = 05/18/15 Pct Recovery = 66% Analysis Date = 05/18/15 Pct Recovery = 66% Analysis Date = 05/13/15 Pct Recovery = 66% Analysis Date = 05/13/15 Pct Recovery = 66% Analysis Date = 05/08/15 Pct Recovery = 66% Analysis Date = 05/08/15 Pct Recovery = 66% Analysis Date = 05/04/15 Pct Recovery = 66% Analysis Date = 05/04/15 Pct Recovery = 66% Analysis Date = 04/29/15 Pct Recovery = 65% Analysis Date = 04/29/15 Pct Recovery = 65% Analysis Date = 04/24/15 Pct Recovery = 65% Analysis Date = 04/24/15 Pct Recovery = 65% Analysis Date = 04/19/15 Pct Recovery = 65% Analysis Date = 04/19/15 Pct Recovery = 65% Analysis Date = 04/14/15 Pct Recovery = 65% Analysis Date = 04/14/15 Pct Recovery = 65% Analysis Date = 04/09/15 Pct Recovery = 65% Analysis Date = 04/09/15 Pct Recovery = 65% Analysis Date = 04/04/15 Pct Recovery = 65% Analysis Date = 04/04/15 Pct Recovery = 65% Analysis Date = 03/30/15 Pct Recovery = 65% Analysis Date = 03/30/15 Pct Recovery = 65% Analysis Date = 03/25/15 Pct Recovery = 65% Analysis Date = 03/25/15 Pct Recovery = 65% Analysis Date = 03/21/15 Pct Recovery = 65% Analysis Date = 03/21/15 Pct Recovery = 65% Analysis Date = 03/16/15 Pct Recovery = 65% Analysis Date = 03/16/15 Pct Recovery = 65% Analysis Date = 03/11/15 Pct Recovery = 65% Analysis Date = 03/11/15 Pct Recovery = 65% Analysis Date = 03/06/15 Pct Recovery = 65% Analysis Date = 03/06/15 Pct Recovery = 65% Analysis Date = 03/01/15 Pct Recovery = 64% Analysis Date = 03/01/15 Pct Recovery = 64% Analysis Date = 02/24/15 Pct Recovery = 64% Analysis Date = 02/24/15 Pct Recovery = 64% Analysis Date = 02/19/15 Pct Recovery = 64% Analysis Date = 02/19/15 Pct Recovery = 64% Analysis Date = 02/14/15 Pct Recovery = 64% Analysis Date = 02/14/15 Pct Recovery = 64% Analysis Date = 02/09/15 Pct Recovery = 64% Analysis Date = 02/09/15 Pct Recovery = 64% Analysis Date = 02/05/15 Pct Recovery = 64% Analysis Date = 02/05/15 Pct Recovery = 64% Analysis Date = 01/31/15 Pct Recovery = 64% Analysis Date = 01/31/15 Pct Recovery = 64% Analysis Date = 01/26/15 Pct Recovery = 64% Analysis Date = 01/26/15 Pct Recovery = 64% Analysis Date = 01/21/15 Pct Recovery = 64% Analysis Date = 01/21/15 Pct Recovery = 64% Analysis Date = 01/16/15 Pct Recovery = 63% Analysis Date = 01/16/15 Pct Recovery = 63% Analysis Date = 01/11/15 Pct Recovery = 63% Analysis Date = 01/11/15 Pct Recovery = 63% Analysis Date = 01/06/15 Pct Recovery = 63% Analysis Date = 01/06/15 Pct Recovery = 63% Analysis Date = 01/01/15 Pct Recovery = 63% Analysis Date = 01/01/15 Pct Recovery = 63% Analysis Date = 12/27/14 Pct Recovery = 63% Analysis Date = 12/27/14 Pct Recovery = 63% Analysis Date = 12/23/14 Pct Recovery = 63% Analysis Date = 12/23/14 Pct Recovery = 63% Analysis Date = 12/18/14 Pct Recovery = 63% Analysis Date = 12/18/14 Pct Recovery = 63% Analysis Date = 12/13/14 Pct Recovery = 63% Analysis Date = 12/13/14 Pct Recovery = 63% Analysis Date = 12/08/14 Pct Recovery = 63% Analysis Date = 12/08/14 Pct Recovery = 63% Analysis Date = 12/03/14 Pct Recovery = 63% Analysis Date = 12/03/14 Pct Recovery = 63% Analysis Date = 11/28/14 Pct Recovery = 62% Analysis Date = 11/28/14 Pct Recovery = 62% Analysis Date = 11/23/14 Pct Recovery = 62% Analysis Date = 11/23/14 Pct Recovery = 62% Analysis Date = 11/18/14 Pct Recovery = 62% Analysis Date = 11/18/14 Pct Recovery = 62% Analysis Date = 11/13/14 Pct Recovery = 62% Analysis Date = 11/13/14 Pct Recovery = 62% Analysis Date = 11/09/14 Pct Recovery = 62% Analysis Date = 11/09/14 Pct Recovery = 62% Analysis Date = 11/04/14 Pct Recovery = 62% Analysis Date = 11/04/14 Pct Recovery = 62% Analysis Date = 10/30/14 Pct Recovery = 62% Analysis Date = 10/30/14 Pct Recovery = 62% Analysis Date = 10/25/14 Pct Recovery = 62% Analysis Date = 10/25/14 Pct Recovery = 62% Analysis Date = 10/20/14 Pct Recovery = 62% Analysis Date = 10/20/14 Pct Recovery = 62% Analysis Date = 10/15/14 Pct Recovery = 62% Analysis Date = 10/15/14 Pct Recovery = 62% Analysis Date = 10/10/14 Pct Recovery = 61% Analysis Date = 10/10/14 Pct Recovery = 61% Analysis Date = 10/05/14 Pct Recovery = 61% Analysis Date = 10/05/14 Pct Recovery = 61% Analysis Date = 09/30/14 Pct Recovery = 61% Analysis Date = 09/30/14 Pct Recovery = 61% Analysis Date = 09/26/14 Pct Recovery = 61% Analysis Date = 09/26/14 Pct Recovery = 61% Analysis Date = 09/21/14 Pct Recovery = 61% Analysis Date = 09/21/14 Pct Recovery = 61% Analysis Date = 09/16/14 Pct Recovery = 61% Analysis Date = 09/16/14 Pct Recovery = 61% Analysis Date = 09/11/14 Pct Recovery = 61% Analysis Date = 09/11/14 Pct Recovery = 61% Analysis Date = 09/06/14 Pct Recovery = 61% Analysis Date = 09/06/14 Pct Recovery = 61% Analysis Date = 09/01/14 Pct Recovery = 61% Analysis Date = 09/01/14 Pct Recovery = 61% Analysis Date = 08/27/14 Pct Recovery = 60% Analysis Date = 08/27/14 Pct Recovery = 60% Analysis Date = 08/22/14 Pct Recovery = 60% Analysis Date = 08/22/14 Pct Recovery = 60% Analysis Date = 08/17/14 Pct Recovery = 60% Analysis Date = 08/17/14 Pct Recovery = 60% Analysis Date = 08/13/14 Pct Recovery = 60% Analysis Date = 08/13/14 Pct Recovery = 60% Analysis Date = 08/08/14 Pct Recovery = 60% Analysis Date = 08/08/14 Pct Recovery = 60% Analysis Date = 08/03/14 Pct Recovery = 60% Analysis Date = 08/03/14 Pct Recovery = 60% Analysis Date = 07/29/14 Pct Recovery = 60% Analysis Date = 07/29/14 Pct Recovery = 60% Analysis Date = 07/24/14 Pct Recovery = 60% Analysis Date = 07/24/14 Pct Recovery = 60% Analysis Date = 07/19/14 Pct Recovery = 60% Analysis Date = 07/19/14 Pct Recovery = 60% Analysis Date = 07/14/14 Pct Recovery = 59% Analysis Date = 07/14/14 Pct Recovery = 59% Analysis Date = 07/09/14 Pct Recovery = 59% Analysis Date = 07/09/14 Pct Recovery = 59% Analysis Date = 07/04/14 Pct Recovery = 59% Analysis Date = 07/04/14 Pct Recovery = 59% Analysis Date = 06/30/14 Pct Recovery = 59% Analysis Date = 06/30/14 Pct Recovery = 59% Analysis Date = 06/25/14 Pct Recovery = 59% Analysis Date = 06/25/14 Pct Recovery = 59% Analysis Date = 06/20/14 Pct Recovery = 59% Analysis Date = 06/20/14 Pct Recovery = 59% Analysis Date = 06/15/14 Pct Recovery = 59% Analysis Date = 06/15/14 Pct Recovery = 59% Analysis Date = 06/10/14 Pct Recovery = 59% Analysis Date = 06/10/14 Pct Recovery = 59% Analysis Date = 06/05/14 Pct Recovery = 59% Analysis Date = 06/05/14 Pct Recovery = 59% Analysis Date = 05/31/14 Pct Recovery = 58% Analysis Date = 05/31/14 Pct Recovery = 58% Analysis Date = 05/26/14 Pct Recovery = 58% Analysis Date = 05/26/14 Pct Recovery = 58% Analysis Date = 05/21/14 Pct Recovery = 58% Analysis Date = 05/21/14 Pct Recovery = 58% Analysis Date = 05/17/14 Pct Recovery = 58% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
METHADONE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 47 68% 16% 64% 10%
Total 47 68% 16% 64% 10%

Sample Statistics
METHADONE

Characteristic N % % Basis
Plotted 47 92% Spiked
Estimated Values 6 12% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 2 4% Spiked
Spiked 51 .  
False Negatives 2 4% 2 out of 51
Not Spiked 64 .  
False Positives 0 0% 0 out of 64

BQS OBSP Determination:
METHOCARBAMOL
METHOD: 2440 , TESTIDCODE: 67501LCM56
Open Data Set

Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 101% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 86% Analysis Date = 01/17/16 SpikeMix = ERA 0406-15-09: 80 µl & ERA 0406-15-07A: 80 µl Pct Recovery = 93% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 80 µl & Abs 051315: 80 µl Pct Recovery = 70% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 80 µl & ERA 0406-15-08: 80 µl Pct Recovery = 70% Analysis Date = 11/04/15 SpikeMix = Abs 052215: 80 µl & Abs 050115: 80 µl Pct Recovery = 86% Analysis Date = 11/18/16 SpikeMix = ERA 04281604: 80 µl & ERA 04281603: 80 µl Pct Recovery = 81% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & ERA 04281604: 80 µl Pct Recovery = 71% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 72% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 70% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 76% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 79% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 91% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 96% Analysis Date = 04/29/15 SpikeMix = ERA 0319-14-05: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 98% Analysis Date = 03/11/15 SpikeMix = ERA 0318-14-02: 15 µl & Abs 041714: 15 µl Pct Recovery = 96% Analysis Date = 02/06/15 SpikeMix = Abs 041814: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 87% Analysis Date = 12/06/14 SpikeMix = ERA 0318-14-02: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 69% Analysis Date = 10/11/14 SpikeMix = ERA 0318-14-02: 60 µl & ERA 0319-14-04: 60 µl Pct Recovery = 59% Analysis Date = 08/21/14 SpikeMix = ERA 0318-14-02: 60 µl & Abs 041714: 60 µl Pct Recovery = 66% Analysis Date = 07/26/14 SpikeMix = ERA 0319-14-05: 60 µl & ERA 0318-14-02: 60 µl Pct Recovery = 76% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 81% Analysis Date = 12/07/14 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 73% Analysis Date = 10/25/14 SpikeMix = Abs 041614: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 77% Analysis Date = 06/22/14 SpikeMix = Abs 041814: 60 µl & Abs 041614: 60 µl Pct Recovery = 98% Analysis Date = 06/11/14 SpikeMix = Abs 041614: 60 µl & Abs 041714: 60 µl Pct Recovery = 75% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-07A: 40 µl & Abs 051315: 40 µl Pct Recovery = 77% Analysis Date = 11/04/15 SpikeMix = ERA 0406-15-07A: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 78% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 76% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 69% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 67% Analysis Date = 02/23/16 SpikeMix = Abs 052215: 40 µl & Abs 050115: 40 µl Pct Recovery = 93% Analysis Date = 07/30/15 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 79% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 99% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 134% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 94% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 85% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 83% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 94% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 71% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 76% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 67% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 54% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 71% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 70% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 78% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 56% Analysis Date = 04/23/14 SpikeMix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.2: 20 µl Pct Recovery = 93% Analysis Date = 12/07/14 SpikeMix = ERA 0318-14-02: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 71% Analysis Date = 11/04/14 SpikeMix = Abs 041814: 8 µl & ERA 0318-14-02: 8 µl Pct Recovery = 88% Analysis Date = 04/30/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 79% Analysis Date = 02/10/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 84% Analysis Date = 10/24/14 SpikeMix = ERA 0319-14-05: 8 µl & Abs 041614: 8 µl Pct Recovery = 73% Analysis Date = 08/30/14 SpikeMix = ERA 0318-14-02: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 77% Analysis Date = 07/20/14 SpikeMix = ERA 0318-14-02: 30 µl & Abs 041714: 30 µl Pct Recovery = 47% Analysis Date = 09/12/14 SpikeMix = Abs 041614: 30 µl & ERA 0319-14-04: 30 µl Pct Recovery = 62% Analysis Date = 07/13/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 83% Analysis Date = 06/28/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 60% Analysis Date = 05/30/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 85% Analysis Date = 05/17/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 46% Analysis Date = 04/27/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 113% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 64% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 97% Analysis Date = 11/24/15 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 93% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-09: 20 µl Pct Recovery = 73% Analysis Date = 11/25/15 SpikeMix = Abs 050115: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 93% Analysis Date = 11/24/15 SpikeMix = ERA 0406-15-09: 20 µl & Abs 050115: 20 µl Pct Recovery = 85% Analysis Date = 08/27/15 SpikeMix = Abs 052215: 20 µl & Abs 050115: 20 µl Pct Recovery = 56% Analysis Date = 08/11/15 SpikeMix = Abs 050115: 20 µl & Abs 051315: 20 µl Pct Recovery = 105% Analysis Date = 07/09/15 SpikeMix = Abs 050115: 20 µl & Abs 052215: 20 µl Pct Recovery = 76% Analysis Date = 06/09/15 SpikeMix = Abs 051315: 20 µl & Abs 050115: 20 µl Pct Recovery = 72% Analysis Date = 01/18/17 Pct Recovery = 87% Analysis Date = 01/13/17 Pct Recovery = 86% Analysis Date = 01/13/17 Pct Recovery = 86% Analysis Date = 01/08/17 Pct Recovery = 86% Analysis Date = 01/08/17 Pct Recovery = 86% Analysis Date = 01/03/17 Pct Recovery = 86% Analysis Date = 01/03/17 Pct Recovery = 86% Analysis Date = 12/29/16 Pct Recovery = 86% Analysis Date = 12/29/16 Pct Recovery = 86% Analysis Date = 12/24/16 Pct Recovery = 86% Analysis Date = 12/24/16 Pct Recovery = 86% Analysis Date = 12/19/16 Pct Recovery = 85% Analysis Date = 12/19/16 Pct Recovery = 85% Analysis Date = 12/14/16 Pct Recovery = 85% Analysis Date = 12/14/16 Pct Recovery = 85% Analysis Date = 12/09/16 Pct Recovery = 85% Analysis Date = 12/09/16 Pct Recovery = 85% Analysis Date = 12/04/16 Pct Recovery = 85% Analysis Date = 12/04/16 Pct Recovery = 85% Analysis Date = 11/29/16 Pct Recovery = 85% Analysis Date = 11/29/16 Pct Recovery = 85% Analysis Date = 11/24/16 Pct Recovery = 84% Analysis Date = 11/24/16 Pct Recovery = 84% Analysis Date = 11/19/16 Pct Recovery = 84% Analysis Date = 11/19/16 Pct Recovery = 84% Analysis Date = 11/14/16 Pct Recovery = 84% Analysis Date = 11/14/16 Pct Recovery = 84% Analysis Date = 11/09/16 Pct Recovery = 84% Analysis Date = 11/09/16 Pct Recovery = 84% Analysis Date = 11/04/16 Pct Recovery = 84% Analysis Date = 11/04/16 Pct Recovery = 84% Analysis Date = 10/30/16 Pct Recovery = 83% Analysis Date = 10/30/16 Pct Recovery = 83% Analysis Date = 10/25/16 Pct Recovery = 83% Analysis Date = 10/25/16 Pct Recovery = 83% Analysis Date = 10/20/16 Pct Recovery = 83% Analysis Date = 10/20/16 Pct Recovery = 83% Analysis Date = 10/15/16 Pct Recovery = 83% Analysis Date = 10/15/16 Pct Recovery = 83% Analysis Date = 10/10/16 Pct Recovery = 83% Analysis Date = 10/10/16 Pct Recovery = 83% Analysis Date = 10/05/16 Pct Recovery = 83% Analysis Date = 10/05/16 Pct Recovery = 83% Analysis Date = 09/30/16 Pct Recovery = 83% Analysis Date = 09/30/16 Pct Recovery = 83% Analysis Date = 09/25/16 Pct Recovery = 82% Analysis Date = 09/25/16 Pct Recovery = 82% Analysis Date = 09/20/16 Pct Recovery = 82% Analysis Date = 09/20/16 Pct Recovery = 82% Analysis Date = 09/15/16 Pct Recovery = 82% Analysis Date = 09/15/16 Pct Recovery = 82% Analysis Date = 09/10/16 Pct Recovery = 82% Analysis Date = 09/10/16 Pct Recovery = 82% Analysis Date = 09/05/16 Pct Recovery = 82% Analysis Date = 09/05/16 Pct Recovery = 82% Analysis Date = 08/31/16 Pct Recovery = 82% Analysis Date = 08/31/16 Pct Recovery = 82% Analysis Date = 08/26/16 Pct Recovery = 82% Analysis Date = 08/26/16 Pct Recovery = 82% Analysis Date = 08/21/16 Pct Recovery = 81% Analysis Date = 08/21/16 Pct Recovery = 81% Analysis Date = 08/16/16 Pct Recovery = 81% Analysis Date = 08/16/16 Pct Recovery = 81% Analysis Date = 08/11/16 Pct Recovery = 81% Analysis Date = 08/11/16 Pct Recovery = 81% Analysis Date = 08/06/16 Pct Recovery = 81% Analysis Date = 08/06/16 Pct Recovery = 81% Analysis Date = 08/01/16 Pct Recovery = 81% Analysis Date = 08/01/16 Pct Recovery = 81% Analysis Date = 07/27/16 Pct Recovery = 81% Analysis Date = 07/27/16 Pct Recovery = 81% Analysis Date = 07/22/16 Pct Recovery = 81% Analysis Date = 07/22/16 Pct Recovery = 81% Analysis Date = 07/17/16 Pct Recovery = 81% Analysis Date = 07/17/16 Pct Recovery = 81% Analysis Date = 07/12/16 Pct Recovery = 81% Analysis Date = 07/12/16 Pct Recovery = 81% Analysis Date = 07/07/16 Pct Recovery = 81% Analysis Date = 07/07/16 Pct Recovery = 81% Analysis Date = 07/02/16 Pct Recovery = 81% Analysis Date = 07/02/16 Pct Recovery = 81% Analysis Date = 06/27/16 Pct Recovery = 81% Analysis Date = 06/27/16 Pct Recovery = 81% Analysis Date = 06/22/16 Pct Recovery = 81% Analysis Date = 06/22/16 Pct Recovery = 81% Analysis Date = 06/17/16 Pct Recovery = 81% Analysis Date = 06/17/16 Pct Recovery = 81% Analysis Date = 06/12/16 Pct Recovery = 81% Analysis Date = 06/12/16 Pct Recovery = 81% Analysis Date = 06/07/16 Pct Recovery = 81% Analysis Date = 06/07/16 Pct Recovery = 81% Analysis Date = 06/02/16 Pct Recovery = 81% Analysis Date = 06/02/16 Pct Recovery = 81% Analysis Date = 05/28/16 Pct Recovery = 81% Analysis Date = 05/28/16 Pct Recovery = 81% Analysis Date = 05/23/16 Pct Recovery = 81% Analysis Date = 05/23/16 Pct Recovery = 81% Analysis Date = 05/18/16 Pct Recovery = 81% Analysis Date = 05/18/16 Pct Recovery = 81% Analysis Date = 05/13/16 Pct Recovery = 81% Analysis Date = 05/13/16 Pct Recovery = 81% Analysis Date = 05/08/16 Pct Recovery = 81% Analysis Date = 05/08/16 Pct Recovery = 81% Analysis Date = 05/03/16 Pct Recovery = 81% Analysis Date = 05/03/16 Pct Recovery = 81% Analysis Date = 04/28/16 Pct Recovery = 80% Analysis Date = 04/28/16 Pct Recovery = 80% Analysis Date = 04/23/16 Pct Recovery = 81% Analysis Date = 04/23/16 Pct Recovery = 81% Analysis Date = 04/18/16 Pct Recovery = 81% Analysis Date = 04/18/16 Pct Recovery = 81% Analysis Date = 04/13/16 Pct Recovery = 81% Analysis Date = 04/13/16 Pct Recovery = 81% Analysis Date = 04/08/16 Pct Recovery = 81% Analysis Date = 04/08/16 Pct Recovery = 81% Analysis Date = 04/03/16 Pct Recovery = 81% Analysis Date = 04/03/16 Pct Recovery = 81% Analysis Date = 03/29/16 Pct Recovery = 81% Analysis Date = 03/29/16 Pct Recovery = 81% Analysis Date = 03/24/16 Pct Recovery = 81% Analysis Date = 03/24/16 Pct Recovery = 81% Analysis Date = 03/19/16 Pct Recovery = 81% Analysis Date = 03/19/16 Pct Recovery = 81% Analysis Date = 03/14/16 Pct Recovery = 81% Analysis Date = 03/14/16 Pct Recovery = 81% Analysis Date = 03/09/16 Pct Recovery = 81% Analysis Date = 03/09/16 Pct Recovery = 81% Analysis Date = 03/04/16 Pct Recovery = 81% Analysis Date = 03/04/16 Pct Recovery = 81% Analysis Date = 02/28/16 Pct Recovery = 81% Analysis Date = 02/28/16 Pct Recovery = 81% Analysis Date = 02/23/16 Pct Recovery = 81% Analysis Date = 02/23/16 Pct Recovery = 81% Analysis Date = 02/18/16 Pct Recovery = 81% Analysis Date = 02/18/16 Pct Recovery = 81% Analysis Date = 02/13/16 Pct Recovery = 81% Analysis Date = 02/13/16 Pct Recovery = 81% Analysis Date = 02/08/16 Pct Recovery = 81% Analysis Date = 02/08/16 Pct Recovery = 81% Analysis Date = 02/03/16 Pct Recovery = 81% Analysis Date = 02/03/16 Pct Recovery = 81% Analysis Date = 01/29/16 Pct Recovery = 81% Analysis Date = 01/29/16 Pct Recovery = 81% Analysis Date = 01/24/16 Pct Recovery = 81% Analysis Date = 01/24/16 Pct Recovery = 81% Analysis Date = 01/19/16 Pct Recovery = 81% Analysis Date = 01/19/16 Pct Recovery = 81% Analysis Date = 01/14/16 Pct Recovery = 81% Analysis Date = 01/14/16 Pct Recovery = 81% Analysis Date = 01/09/16 Pct Recovery = 81% Analysis Date = 01/09/16 Pct Recovery = 81% Analysis Date = 01/04/16 Pct Recovery = 81% Analysis Date = 01/04/16 Pct Recovery = 81% Analysis Date = 12/30/15 Pct Recovery = 82% Analysis Date = 12/30/15 Pct Recovery = 82% Analysis Date = 12/25/15 Pct Recovery = 82% Analysis Date = 12/25/15 Pct Recovery = 82% Analysis Date = 12/20/15 Pct Recovery = 82% Analysis Date = 12/20/15 Pct Recovery = 82% Analysis Date = 12/15/15 Pct Recovery = 82% Analysis Date = 12/15/15 Pct Recovery = 82% Analysis Date = 12/10/15 Pct Recovery = 82% Analysis Date = 12/10/15 Pct Recovery = 82% Analysis Date = 12/05/15 Pct Recovery = 82% Analysis Date = 12/05/15 Pct Recovery = 82% Analysis Date = 11/30/15 Pct Recovery = 82% Analysis Date = 11/30/15 Pct Recovery = 82% Analysis Date = 11/25/15 Pct Recovery = 82% Analysis Date = 11/25/15 Pct Recovery = 82% Analysis Date = 11/20/15 Pct Recovery = 82% Analysis Date = 11/20/15 Pct Recovery = 82% Analysis Date = 11/15/15 Pct Recovery = 82% Analysis Date = 11/15/15 Pct Recovery = 82% Analysis Date = 11/10/15 Pct Recovery = 82% Analysis Date = 11/10/15 Pct Recovery = 82% Analysis Date = 11/05/15 Pct Recovery = 82% Analysis Date = 11/05/15 Pct Recovery = 82% Analysis Date = 10/31/15 Pct Recovery = 82% Analysis Date = 10/31/15 Pct Recovery = 82% Analysis Date = 10/26/15 Pct Recovery = 82% Analysis Date = 10/26/15 Pct Recovery = 82% Analysis Date = 10/21/15 Pct Recovery = 82% Analysis Date = 10/21/15 Pct Recovery = 82% Analysis Date = 10/16/15 Pct Recovery = 82% Analysis Date = 10/16/15 Pct Recovery = 82% Analysis Date = 10/11/15 Pct Recovery = 82% Analysis Date = 10/11/15 Pct Recovery = 82% Analysis Date = 10/06/15 Pct Recovery = 82% Analysis Date = 10/06/15 Pct Recovery = 82% Analysis Date = 10/01/15 Pct Recovery = 82% Analysis Date = 10/01/15 Pct Recovery = 82% Analysis Date = 09/26/15 Pct Recovery = 82% Analysis Date = 09/26/15 Pct Recovery = 82% Analysis Date = 09/21/15 Pct Recovery = 82% Analysis Date = 09/21/15 Pct Recovery = 82% Analysis Date = 09/16/15 Pct Recovery = 82% Analysis Date = 09/16/15 Pct Recovery = 82% Analysis Date = 09/11/15 Pct Recovery = 82% Analysis Date = 09/11/15 Pct Recovery = 82% Analysis Date = 09/05/15 Pct Recovery = 82% Analysis Date = 09/05/15 Pct Recovery = 82% Analysis Date = 08/31/15 Pct Recovery = 82% Analysis Date = 08/31/15 Pct Recovery = 82% Analysis Date = 08/26/15 Pct Recovery = 82% Analysis Date = 08/26/15 Pct Recovery = 82% Analysis Date = 08/21/15 Pct Recovery = 82% Analysis Date = 08/21/15 Pct Recovery = 82% Analysis Date = 08/16/15 Pct Recovery = 81% Analysis Date = 08/16/15 Pct Recovery = 81% Analysis Date = 08/11/15 Pct Recovery = 81% Analysis Date = 08/11/15 Pct Recovery = 81% Analysis Date = 08/06/15 Pct Recovery = 81% Analysis Date = 08/06/15 Pct Recovery = 81% Analysis Date = 08/01/15 Pct Recovery = 81% Analysis Date = 08/01/15 Pct Recovery = 81% Analysis Date = 07/27/15 Pct Recovery = 81% Analysis Date = 07/27/15 Pct Recovery = 81% Analysis Date = 07/22/15 Pct Recovery = 81% Analysis Date = 07/22/15 Pct Recovery = 81% Analysis Date = 07/17/15 Pct Recovery = 81% Analysis Date = 07/17/15 Pct Recovery = 81% Analysis Date = 07/12/15 Pct Recovery = 81% Analysis Date = 07/12/15 Pct Recovery = 81% Analysis Date = 07/07/15 Pct Recovery = 81% Analysis Date = 07/07/15 Pct Recovery = 81% Analysis Date = 07/02/15 Pct Recovery = 81% Analysis Date = 07/02/15 Pct Recovery = 81% Analysis Date = 06/27/15 Pct Recovery = 81% Analysis Date = 06/27/15 Pct Recovery = 81% Analysis Date = 06/22/15 Pct Recovery = 81% Analysis Date = 06/22/15 Pct Recovery = 81% Analysis Date = 06/17/15 Pct Recovery = 81% Analysis Date = 06/17/15 Pct Recovery = 81% Analysis Date = 06/12/15 Pct Recovery = 80% Analysis Date = 06/12/15 Pct Recovery = 80% Analysis Date = 06/07/15 Pct Recovery = 80% Analysis Date = 06/07/15 Pct Recovery = 80% Analysis Date = 06/02/15 Pct Recovery = 80% Analysis Date = 06/02/15 Pct Recovery = 80% Analysis Date = 05/28/15 Pct Recovery = 80% Analysis Date = 05/28/15 Pct Recovery = 80% Analysis Date = 05/23/15 Pct Recovery = 80% Analysis Date = 05/23/15 Pct Recovery = 80% Analysis Date = 05/18/15 Pct Recovery = 80% Analysis Date = 05/18/15 Pct Recovery = 80% Analysis Date = 05/13/15 Pct Recovery = 80% Analysis Date = 05/13/15 Pct Recovery = 80% Analysis Date = 05/08/15 Pct Recovery = 80% Analysis Date = 05/08/15 Pct Recovery = 80% Analysis Date = 05/03/15 Pct Recovery = 80% Analysis Date = 05/03/15 Pct Recovery = 80% Analysis Date = 04/28/15 Pct Recovery = 79% Analysis Date = 04/28/15 Pct Recovery = 79% Analysis Date = 04/23/15 Pct Recovery = 79% Analysis Date = 04/23/15 Pct Recovery = 79% Analysis Date = 04/18/15 Pct Recovery = 79% Analysis Date = 04/18/15 Pct Recovery = 79% Analysis Date = 04/13/15 Pct Recovery = 79% Analysis Date = 04/13/15 Pct Recovery = 79% Analysis Date = 04/08/15 Pct Recovery = 79% Analysis Date = 04/08/15 Pct Recovery = 79% Analysis Date = 04/03/15 Pct Recovery = 79% Analysis Date = 04/03/15 Pct Recovery = 79% Analysis Date = 03/29/15 Pct Recovery = 79% Analysis Date = 03/29/15 Pct Recovery = 79% Analysis Date = 03/24/15 Pct Recovery = 79% Analysis Date = 03/24/15 Pct Recovery = 79% Analysis Date = 03/19/15 Pct Recovery = 79% Analysis Date = 03/19/15 Pct Recovery = 79% Analysis Date = 03/14/15 Pct Recovery = 78% Analysis Date = 03/14/15 Pct Recovery = 78% Analysis Date = 03/09/15 Pct Recovery = 78% Analysis Date = 03/09/15 Pct Recovery = 78% Analysis Date = 03/04/15 Pct Recovery = 78% Analysis Date = 03/04/15 Pct Recovery = 78% Analysis Date = 02/27/15 Pct Recovery = 78% Analysis Date = 02/27/15 Pct Recovery = 78% Analysis Date = 02/22/15 Pct Recovery = 78% Analysis Date = 02/22/15 Pct Recovery = 78% Analysis Date = 02/17/15 Pct Recovery = 78% Analysis Date = 02/17/15 Pct Recovery = 78% Analysis Date = 02/12/15 Pct Recovery = 78% Analysis Date = 02/12/15 Pct Recovery = 78% Analysis Date = 02/07/15 Pct Recovery = 78% Analysis Date = 02/07/15 Pct Recovery = 78% Analysis Date = 02/02/15 Pct Recovery = 78% Analysis Date = 02/02/15 Pct Recovery = 78% Analysis Date = 01/28/15 Pct Recovery = 77% Analysis Date = 01/28/15 Pct Recovery = 77% Analysis Date = 01/23/15 Pct Recovery = 77% Analysis Date = 01/23/15 Pct Recovery = 77% Analysis Date = 01/18/15 Pct Recovery = 77% Analysis Date = 01/18/15 Pct Recovery = 77% Analysis Date = 01/13/15 Pct Recovery = 77% Analysis Date = 01/13/15 Pct Recovery = 77% Analysis Date = 01/08/15 Pct Recovery = 77% Analysis Date = 01/08/15 Pct Recovery = 77% Analysis Date = 01/03/15 Pct Recovery = 77% Analysis Date = 01/03/15 Pct Recovery = 77% Analysis Date = 12/29/14 Pct Recovery = 77% Analysis Date = 12/29/14 Pct Recovery = 77% Analysis Date = 12/24/14 Pct Recovery = 77% Analysis Date = 12/24/14 Pct Recovery = 77% Analysis Date = 12/19/14 Pct Recovery = 77% Analysis Date = 12/19/14 Pct Recovery = 77% Analysis Date = 12/14/14 Pct Recovery = 76% Analysis Date = 12/14/14 Pct Recovery = 76% Analysis Date = 12/09/14 Pct Recovery = 76% Analysis Date = 12/09/14 Pct Recovery = 76% Analysis Date = 12/04/14 Pct Recovery = 76% Analysis Date = 12/04/14 Pct Recovery = 76% Analysis Date = 11/29/14 Pct Recovery = 76% Analysis Date = 11/29/14 Pct Recovery = 76% Analysis Date = 11/24/14 Pct Recovery = 76% Analysis Date = 11/24/14 Pct Recovery = 76% Analysis Date = 11/19/14 Pct Recovery = 76% Analysis Date = 11/19/14 Pct Recovery = 76% Analysis Date = 11/14/14 Pct Recovery = 76% Analysis Date = 11/14/14 Pct Recovery = 76% Analysis Date = 11/09/14 Pct Recovery = 76% Analysis Date = 11/09/14 Pct Recovery = 76% Analysis Date = 11/04/14 Pct Recovery = 76% Analysis Date = 11/04/14 Pct Recovery = 76% Analysis Date = 10/30/14 Pct Recovery = 76% Analysis Date = 10/30/14 Pct Recovery = 76% Analysis Date = 10/25/14 Pct Recovery = 75% Analysis Date = 10/25/14 Pct Recovery = 75% Analysis Date = 10/20/14 Pct Recovery = 75% Analysis Date = 10/20/14 Pct Recovery = 75% Analysis Date = 10/15/14 Pct Recovery = 75% Analysis Date = 10/15/14 Pct Recovery = 75% Analysis Date = 10/10/14 Pct Recovery = 75% Analysis Date = 10/10/14 Pct Recovery = 75% Analysis Date = 10/05/14 Pct Recovery = 75% Analysis Date = 10/05/14 Pct Recovery = 75% Analysis Date = 09/30/14 Pct Recovery = 75% Analysis Date = 09/30/14 Pct Recovery = 75% Analysis Date = 09/25/14 Pct Recovery = 75% Analysis Date = 09/25/14 Pct Recovery = 75% Analysis Date = 09/20/14 Pct Recovery = 75% Analysis Date = 09/20/14 Pct Recovery = 75% Analysis Date = 09/15/14 Pct Recovery = 75% Analysis Date = 09/15/14 Pct Recovery = 75% Analysis Date = 09/10/14 Pct Recovery = 74% Analysis Date = 09/10/14 Pct Recovery = 74% Analysis Date = 09/05/14 Pct Recovery = 74% Analysis Date = 09/05/14 Pct Recovery = 74% Analysis Date = 08/31/14 Pct Recovery = 74% Analysis Date = 08/31/14 Pct Recovery = 74% Analysis Date = 08/26/14 Pct Recovery = 74% Analysis Date = 08/26/14 Pct Recovery = 74% Analysis Date = 08/21/14 Pct Recovery = 74% Analysis Date = 08/21/14 Pct Recovery = 74% Analysis Date = 08/16/14 Pct Recovery = 74% Analysis Date = 08/16/14 Pct Recovery = 74% Analysis Date = 08/11/14 Pct Recovery = 74% Analysis Date = 08/11/14 Pct Recovery = 74% Analysis Date = 08/06/14 Pct Recovery = 74% Analysis Date = 08/06/14 Pct Recovery = 74% Analysis Date = 08/01/14 Pct Recovery = 73% Analysis Date = 08/01/14 Pct Recovery = 73% Analysis Date = 07/27/14 Pct Recovery = 73% Analysis Date = 07/27/14 Pct Recovery = 73% Analysis Date = 07/22/14 Pct Recovery = 73% Analysis Date = 07/22/14 Pct Recovery = 73% Analysis Date = 07/17/14 Pct Recovery = 73% Analysis Date = 07/17/14 Pct Recovery = 73% Analysis Date = 07/12/14 Pct Recovery = 73% Analysis Date = 07/12/14 Pct Recovery = 73% Analysis Date = 07/07/14 Pct Recovery = 73% Analysis Date = 07/07/14 Pct Recovery = 73% Analysis Date = 07/02/14 Pct Recovery = 73% Analysis Date = 07/02/14 Pct Recovery = 73% Analysis Date = 06/27/14 Pct Recovery = 73% Analysis Date = 06/27/14 Pct Recovery = 73% Analysis Date = 06/22/14 Pct Recovery = 72% Analysis Date = 06/22/14 Pct Recovery = 72% Analysis Date = 06/17/14 Pct Recovery = 72% Analysis Date = 06/17/14 Pct Recovery = 72% Analysis Date = 06/12/14 Pct Recovery = 72% Analysis Date = 06/12/14 Pct Recovery = 72% Analysis Date = 06/07/14 Pct Recovery = 72% Analysis Date = 06/07/14 Pct Recovery = 72% Analysis Date = 06/02/14 Pct Recovery = 72% Analysis Date = 06/02/14 Pct Recovery = 72% Analysis Date = 05/28/14 Pct Recovery = 72% Analysis Date = 05/28/14 Pct Recovery = 72% Analysis Date = 05/23/14 Pct Recovery = 72% Analysis Date = 05/23/14 Pct Recovery = 72% Analysis Date = 05/18/14 Pct Recovery = 72% Analysis Date = 05/18/14 Pct Recovery = 72% Analysis Date = 05/13/14 Pct Recovery = 72% Analysis Date = 05/13/14 Pct Recovery = 72% Analysis Date = 05/08/14 Pct Recovery = 71% Analysis Date = 05/08/14 Pct Recovery = 71% Analysis Date = 05/03/14 Pct Recovery = 71% Analysis Date = 05/03/14 Pct Recovery = 71% Analysis Date = 04/28/14 Pct Recovery = 71% Analysis Date = 04/28/14 Pct Recovery = 71% Analysis Date = 04/23/14 Pct Recovery = 71% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
METHOCARBAMOL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 71 80% 15% 77% 15%
Total 71 80% 15% 77% 15%

Sample Statistics
METHOCARBAMOL

Characteristic N % % Basis
Plotted 71 91% Spiked
Estimated Values 9 12% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 3 4% Spiked
Spiked 78 .  
False Negatives 4 5% 4 out of 78
Not Spiked 37 .  
False Positives 1 3% 1 out of 37

BQS OBSP Determination:
METHOTREXATE
METHOD: 2440 , TESTIDCODE: 67525LCM56
Open Data Set

Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 35% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 32% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 57% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 59% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 80 µl & ERA 0406-15-08: 80 µl Pct Recovery = 30% Analysis Date = 11/04/15 SpikeMix = Abs 052215: 80 µl & Abs 050115: 80 µl Pct Recovery = 62% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 21% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 21% Analysis Date = 09/24/16 SpikeMix = Crescent EN160610015: 80 µl & Abs 061416: 80 µl Pct Recovery = 33% Analysis Date = 09/24/16 SpikeMix = Abs 061416: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 31% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 51% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 51% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 57% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 46% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 51% Analysis Date = 12/07/14 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 48% Analysis Date = 10/25/14 SpikeMix = Abs 041614: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 52% Analysis Date = 06/22/14 SpikeMix = Abs 041814: 60 µl & Abs 041614: 60 µl Pct Recovery = 93% Analysis Date = 06/11/14 SpikeMix = Abs 041614: 60 µl & Abs 041714: 60 µl Pct Recovery = 84% Analysis Date = 04/29/15 SpikeMix = ERA 0319-14-05: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 68% Analysis Date = 03/11/15 SpikeMix = ERA 0318-14-02: 15 µl & Abs 041714: 15 µl Pct Recovery = 73% Analysis Date = 02/06/15 SpikeMix = Abs 041814: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 52% Analysis Date = 12/06/14 SpikeMix = ERA 0318-14-02: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 57% Analysis Date = 10/11/14 SpikeMix = ERA 0318-14-02: 60 µl & ERA 0319-14-04: 60 µl Pct Recovery = 87% Analysis Date = 08/21/14 SpikeMix = ERA 0318-14-02: 60 µl & Abs 041714: 60 µl Pct Recovery = 92% Analysis Date = 07/26/14 SpikeMix = ERA 0319-14-05: 60 µl & ERA 0318-14-02: 60 µl Pct Recovery = 86% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 49% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 50% Analysis Date = 07/31/15 SpikeMix = ERA 0406-15-09: 40 µl & Abs 050115: 40 µl Pct Recovery = 63% Analysis Date = 07/30/15 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 70% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 49% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 44% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 35% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 34% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 43% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 51% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 56% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 53% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 40% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 38% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 45% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 53% Analysis Date = 04/30/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 53% Analysis Date = 02/10/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 73% Analysis Date = 10/24/14 SpikeMix = ERA 0319-14-05: 8 µl & Abs 041614: 8 µl Pct Recovery = 63% Analysis Date = 12/07/14 SpikeMix = ERA 0318-14-02: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 76% Analysis Date = 11/04/14 SpikeMix = Abs 041814: 8 µl & ERA 0318-14-02: 8 µl Pct Recovery = 84% Analysis Date = 09/12/14 SpikeMix = Abs 041614: 30 µl & ERA 0319-14-04: 30 µl Pct Recovery = 68% Analysis Date = 07/13/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 43% Analysis Date = 06/28/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 58% Analysis Date = 05/30/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 66% Analysis Date = 05/17/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 71% Analysis Date = 10/10/14 SpikeMix = Abs 041814: 30 µl & ERA 0318-14-02: 30 µl Pct Recovery = 92% Analysis Date = 08/30/14 SpikeMix = ERA 0318-14-02: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 79% Analysis Date = 07/20/14 SpikeMix = ERA 0318-14-02: 30 µl & Abs 041714: 30 µl Pct Recovery = 67% Analysis Date = 11/25/15 SpikeMix = Abs 050115: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 58% Analysis Date = 11/24/15 SpikeMix = ERA 0406-15-09: 20 µl & Abs 050115: 20 µl Pct Recovery = 39% Analysis Date = 08/11/15 SpikeMix = Abs 050115: 20 µl & Abs 051315: 20 µl Pct Recovery = 41% Analysis Date = 07/09/15 SpikeMix = Abs 050115: 20 µl & Abs 052215: 20 µl Pct Recovery = 58% Analysis Date = 06/09/15 SpikeMix = Abs 051315: 20 µl & Abs 050115: 20 µl Pct Recovery = 44% Analysis Date = 01/18/17 Pct Recovery = 41% Analysis Date = 01/14/17 Pct Recovery = 41% Analysis Date = 01/14/17 Pct Recovery = 41% Analysis Date = 01/09/17 Pct Recovery = 42% Analysis Date = 01/09/17 Pct Recovery = 42% Analysis Date = 01/04/17 Pct Recovery = 42% Analysis Date = 01/04/17 Pct Recovery = 42% Analysis Date = 12/30/16 Pct Recovery = 42% Analysis Date = 12/30/16 Pct Recovery = 42% Analysis Date = 12/25/16 Pct Recovery = 42% Analysis Date = 12/25/16 Pct Recovery = 42% Analysis Date = 12/20/16 Pct Recovery = 42% Analysis Date = 12/20/16 Pct Recovery = 42% Analysis Date = 12/15/16 Pct Recovery = 42% Analysis Date = 12/15/16 Pct Recovery = 42% Analysis Date = 12/10/16 Pct Recovery = 42% Analysis Date = 12/10/16 Pct Recovery = 42% Analysis Date = 12/05/16 Pct Recovery = 42% Analysis Date = 12/05/16 Pct Recovery = 42% Analysis Date = 12/01/16 Pct Recovery = 42% Analysis Date = 12/01/16 Pct Recovery = 42% Analysis Date = 11/26/16 Pct Recovery = 42% Analysis Date = 11/26/16 Pct Recovery = 42% Analysis Date = 11/21/16 Pct Recovery = 42% Analysis Date = 11/21/16 Pct Recovery = 42% Analysis Date = 11/16/16 Pct Recovery = 42% Analysis Date = 11/16/16 Pct Recovery = 42% Analysis Date = 11/11/16 Pct Recovery = 42% Analysis Date = 11/11/16 Pct Recovery = 42% Analysis Date = 11/06/16 Pct Recovery = 43% Analysis Date = 11/06/16 Pct Recovery = 43% Analysis Date = 11/01/16 Pct Recovery = 43% Analysis Date = 11/01/16 Pct Recovery = 43% Analysis Date = 10/27/16 Pct Recovery = 43% Analysis Date = 10/27/16 Pct Recovery = 43% Analysis Date = 10/22/16 Pct Recovery = 43% Analysis Date = 10/22/16 Pct Recovery = 43% Analysis Date = 10/18/16 Pct Recovery = 43% Analysis Date = 10/18/16 Pct Recovery = 43% Analysis Date = 10/13/16 Pct Recovery = 43% Analysis Date = 10/13/16 Pct Recovery = 43% Analysis Date = 10/08/16 Pct Recovery = 43% Analysis Date = 10/08/16 Pct Recovery = 43% Analysis Date = 10/03/16 Pct Recovery = 43% Analysis Date = 10/03/16 Pct Recovery = 43% Analysis Date = 09/28/16 Pct Recovery = 43% Analysis Date = 09/28/16 Pct Recovery = 43% Analysis Date = 09/23/16 Pct Recovery = 43% Analysis Date = 09/23/16 Pct Recovery = 43% Analysis Date = 09/18/16 Pct Recovery = 43% Analysis Date = 09/18/16 Pct Recovery = 43% Analysis Date = 09/13/16 Pct Recovery = 43% Analysis Date = 09/13/16 Pct Recovery = 43% Analysis Date = 09/08/16 Pct Recovery = 44% Analysis Date = 09/08/16 Pct Recovery = 44% Analysis Date = 09/04/16 Pct Recovery = 44% Analysis Date = 09/04/16 Pct Recovery = 44% Analysis Date = 08/30/16 Pct Recovery = 44% Analysis Date = 08/30/16 Pct Recovery = 44% Analysis Date = 08/25/16 Pct Recovery = 44% Analysis Date = 08/25/16 Pct Recovery = 44% Analysis Date = 08/20/16 Pct Recovery = 44% Analysis Date = 08/20/16 Pct Recovery = 44% Analysis Date = 08/15/16 Pct Recovery = 44% Analysis Date = 08/15/16 Pct Recovery = 44% Analysis Date = 08/10/16 Pct Recovery = 44% Analysis Date = 08/10/16 Pct Recovery = 44% Analysis Date = 08/05/16 Pct Recovery = 44% Analysis Date = 08/05/16 Pct Recovery = 44% Analysis Date = 07/31/16 Pct Recovery = 44% Analysis Date = 07/31/16 Pct Recovery = 44% Analysis Date = 07/26/16 Pct Recovery = 44% Analysis Date = 07/26/16 Pct Recovery = 44% Analysis Date = 07/22/16 Pct Recovery = 44% Analysis Date = 07/22/16 Pct Recovery = 44% Analysis Date = 07/17/16 Pct Recovery = 45% Analysis Date = 07/17/16 Pct Recovery = 45% Analysis Date = 07/12/16 Pct Recovery = 45% Analysis Date = 07/12/16 Pct Recovery = 45% Analysis Date = 07/07/16 Pct Recovery = 45% Analysis Date = 07/07/16 Pct Recovery = 45% Analysis Date = 07/02/16 Pct Recovery = 45% Analysis Date = 07/02/16 Pct Recovery = 45% Analysis Date = 06/27/16 Pct Recovery = 45% Analysis Date = 06/27/16 Pct Recovery = 45% Analysis Date = 06/22/16 Pct Recovery = 45% Analysis Date = 06/22/16 Pct Recovery = 45% Analysis Date = 06/17/16 Pct Recovery = 46% Analysis Date = 06/17/16 Pct Recovery = 46% Analysis Date = 06/12/16 Pct Recovery = 46% Analysis Date = 06/12/16 Pct Recovery = 46% Analysis Date = 06/08/16 Pct Recovery = 46% Analysis Date = 06/08/16 Pct Recovery = 46% Analysis Date = 06/03/16 Pct Recovery = 46% Analysis Date = 06/03/16 Pct Recovery = 46% Analysis Date = 05/29/16 Pct Recovery = 46% Analysis Date = 05/29/16 Pct Recovery = 46% Analysis Date = 05/24/16 Pct Recovery = 46% Analysis Date = 05/24/16 Pct Recovery = 46% Analysis Date = 05/19/16 Pct Recovery = 46% Analysis Date = 05/19/16 Pct Recovery = 46% Analysis Date = 05/14/16 Pct Recovery = 47% Analysis Date = 05/14/16 Pct Recovery = 47% Analysis Date = 05/09/16 Pct Recovery = 47% Analysis Date = 05/09/16 Pct Recovery = 47% Analysis Date = 05/04/16 Pct Recovery = 47% Analysis Date = 05/04/16 Pct Recovery = 47% Analysis Date = 04/29/16 Pct Recovery = 47% Analysis Date = 04/29/16 Pct Recovery = 47% Analysis Date = 04/25/16 Pct Recovery = 47% Analysis Date = 04/25/16 Pct Recovery = 47% Analysis Date = 04/20/16 Pct Recovery = 47% Analysis Date = 04/20/16 Pct Recovery = 47% Analysis Date = 04/15/16 Pct Recovery = 47% Analysis Date = 04/15/16 Pct Recovery = 47% Analysis Date = 04/10/16 Pct Recovery = 48% Analysis Date = 04/10/16 Pct Recovery = 48% Analysis Date = 04/05/16 Pct Recovery = 48% Analysis Date = 04/05/16 Pct Recovery = 48% Analysis Date = 03/31/16 Pct Recovery = 48% Analysis Date = 03/31/16 Pct Recovery = 48% Analysis Date = 03/26/16 Pct Recovery = 48% Analysis Date = 03/26/16 Pct Recovery = 48% Analysis Date = 03/21/16 Pct Recovery = 48% Analysis Date = 03/21/16 Pct Recovery = 48% Analysis Date = 03/16/16 Pct Recovery = 48% Analysis Date = 03/16/16 Pct Recovery = 48% Analysis Date = 03/12/16 Pct Recovery = 48% Analysis Date = 03/12/16 Pct Recovery = 48% Analysis Date = 03/07/16 Pct Recovery = 49% Analysis Date = 03/07/16 Pct Recovery = 49% Analysis Date = 03/02/16 Pct Recovery = 49% Analysis Date = 03/02/16 Pct Recovery = 49% Analysis Date = 02/26/16 Pct Recovery = 49% Analysis Date = 02/26/16 Pct Recovery = 49% Analysis Date = 02/21/16 Pct Recovery = 49% Analysis Date = 02/21/16 Pct Recovery = 49% Analysis Date = 02/16/16 Pct Recovery = 49% Analysis Date = 02/16/16 Pct Recovery = 49% Analysis Date = 02/11/16 Pct Recovery = 49% Analysis Date = 02/11/16 Pct Recovery = 49% Analysis Date = 02/06/16 Pct Recovery = 50% Analysis Date = 02/06/16 Pct Recovery = 50% Analysis Date = 02/01/16 Pct Recovery = 50% Analysis Date = 02/01/16 Pct Recovery = 50% Analysis Date = 01/28/16 Pct Recovery = 50% Analysis Date = 01/28/16 Pct Recovery = 50% Analysis Date = 01/23/16 Pct Recovery = 50% Analysis Date = 01/23/16 Pct Recovery = 50% Analysis Date = 01/18/16 Pct Recovery = 50% Analysis Date = 01/18/16 Pct Recovery = 50% Analysis Date = 01/13/16 Pct Recovery = 50% Analysis Date = 01/13/16 Pct Recovery = 50% Analysis Date = 01/08/16 Pct Recovery = 50% Analysis Date = 01/08/16 Pct Recovery = 50% Analysis Date = 01/03/16 Pct Recovery = 51% Analysis Date = 01/03/16 Pct Recovery = 51% Analysis Date = 12/29/15 Pct Recovery = 51% Analysis Date = 12/29/15 Pct Recovery = 51% Analysis Date = 12/24/15 Pct Recovery = 51% Analysis Date = 12/24/15 Pct Recovery = 51% Analysis Date = 12/19/15 Pct Recovery = 51% Analysis Date = 12/19/15 Pct Recovery = 51% Analysis Date = 12/15/15 Pct Recovery = 51% Analysis Date = 12/15/15 Pct Recovery = 51% Analysis Date = 12/10/15 Pct Recovery = 51% Analysis Date = 12/10/15 Pct Recovery = 51% Analysis Date = 12/05/15 Pct Recovery = 51% Analysis Date = 12/05/15 Pct Recovery = 51% Analysis Date = 11/30/15 Pct Recovery = 52% Analysis Date = 11/30/15 Pct Recovery = 52% Analysis Date = 11/25/15 Pct Recovery = 52% Analysis Date = 11/25/15 Pct Recovery = 52% Analysis Date = 11/20/15 Pct Recovery = 52% Analysis Date = 11/20/15 Pct Recovery = 52% Analysis Date = 11/15/15 Pct Recovery = 52% Analysis Date = 11/15/15 Pct Recovery = 52% Analysis Date = 11/10/15 Pct Recovery = 52% Analysis Date = 11/10/15 Pct Recovery = 52% Analysis Date = 11/05/15 Pct Recovery = 52% Analysis Date = 11/05/15 Pct Recovery = 52% Analysis Date = 11/01/15 Pct Recovery = 52% Analysis Date = 11/01/15 Pct Recovery = 52% Analysis Date = 10/27/15 Pct Recovery = 53% Analysis Date = 10/27/15 Pct Recovery = 53% Analysis Date = 10/22/15 Pct Recovery = 53% Analysis Date = 10/22/15 Pct Recovery = 53% Analysis Date = 10/17/15 Pct Recovery = 53% Analysis Date = 10/17/15 Pct Recovery = 53% Analysis Date = 10/12/15 Pct Recovery = 53% Analysis Date = 10/12/15 Pct Recovery = 53% Analysis Date = 10/07/15 Pct Recovery = 53% Analysis Date = 10/07/15 Pct Recovery = 53% Analysis Date = 10/02/15 Pct Recovery = 53% Analysis Date = 10/02/15 Pct Recovery = 53% Analysis Date = 09/27/15 Pct Recovery = 54% Analysis Date = 09/27/15 Pct Recovery = 54% Analysis Date = 09/22/15 Pct Recovery = 54% Analysis Date = 09/22/15 Pct Recovery = 54% Analysis Date = 09/17/15 Pct Recovery = 54% Analysis Date = 09/17/15 Pct Recovery = 54% Analysis Date = 09/13/15 Pct Recovery = 54% Analysis Date = 09/13/15 Pct Recovery = 54% Analysis Date = 09/08/15 Pct Recovery = 54% Analysis Date = 09/08/15 Pct Recovery = 54% Analysis Date = 09/03/15 Pct Recovery = 54% Analysis Date = 09/03/15 Pct Recovery = 54% Analysis Date = 08/29/15 Pct Recovery = 54% Analysis Date = 08/29/15 Pct Recovery = 54% Analysis Date = 08/24/15 Pct Recovery = 55% Analysis Date = 08/24/15 Pct Recovery = 55% Analysis Date = 08/19/15 Pct Recovery = 55% Analysis Date = 08/19/15 Pct Recovery = 55% Analysis Date = 08/14/15 Pct Recovery = 55% Analysis Date = 08/14/15 Pct Recovery = 55% Analysis Date = 08/09/15 Pct Recovery = 55% Analysis Date = 08/09/15 Pct Recovery = 55% Analysis Date = 08/04/15 Pct Recovery = 55% Analysis Date = 08/04/15 Pct Recovery = 55% Analysis Date = 07/31/15 Pct Recovery = 55% Analysis Date = 07/31/15 Pct Recovery = 55% Analysis Date = 07/26/15 Pct Recovery = 56% Analysis Date = 07/26/15 Pct Recovery = 56% Analysis Date = 07/21/15 Pct Recovery = 56% Analysis Date = 07/21/15 Pct Recovery = 56% Analysis Date = 07/16/15 Pct Recovery = 56% Analysis Date = 07/16/15 Pct Recovery = 56% Analysis Date = 07/11/15 Pct Recovery = 56% Analysis Date = 07/11/15 Pct Recovery = 56% Analysis Date = 07/06/15 Pct Recovery = 57% Analysis Date = 07/06/15 Pct Recovery = 57% Analysis Date = 07/01/15 Pct Recovery = 57% Analysis Date = 07/01/15 Pct Recovery = 57% Analysis Date = 06/26/15 Pct Recovery = 57% Analysis Date = 06/26/15 Pct Recovery = 57% Analysis Date = 06/21/15 Pct Recovery = 57% Analysis Date = 06/21/15 Pct Recovery = 57% Analysis Date = 06/17/15 Pct Recovery = 58% Analysis Date = 06/17/15 Pct Recovery = 58% Analysis Date = 06/12/15 Pct Recovery = 58% Analysis Date = 06/12/15 Pct Recovery = 58% Analysis Date = 06/07/15 Pct Recovery = 58% Analysis Date = 06/07/15 Pct Recovery = 58% Analysis Date = 06/02/15 Pct Recovery = 58% Analysis Date = 06/02/15 Pct Recovery = 58% Analysis Date = 05/28/15 Pct Recovery = 59% Analysis Date = 05/28/15 Pct Recovery = 59% Analysis Date = 05/23/15 Pct Recovery = 59% Analysis Date = 05/23/15 Pct Recovery = 59% Analysis Date = 05/18/15 Pct Recovery = 59% Analysis Date = 05/18/15 Pct Recovery = 59% Analysis Date = 05/13/15 Pct Recovery = 59% Analysis Date = 05/13/15 Pct Recovery = 59% Analysis Date = 05/08/15 Pct Recovery = 60% Analysis Date = 05/08/15 Pct Recovery = 60% Analysis Date = 05/04/15 Pct Recovery = 60% Analysis Date = 05/04/15 Pct Recovery = 60% Analysis Date = 04/29/15 Pct Recovery = 60% Analysis Date = 04/29/15 Pct Recovery = 60% Analysis Date = 04/24/15 Pct Recovery = 60% Analysis Date = 04/24/15 Pct Recovery = 60% Analysis Date = 04/19/15 Pct Recovery = 61% Analysis Date = 04/19/15 Pct Recovery = 61% Analysis Date = 04/14/15 Pct Recovery = 61% Analysis Date = 04/14/15 Pct Recovery = 61% Analysis Date = 04/09/15 Pct Recovery = 61% Analysis Date = 04/09/15 Pct Recovery = 61% Analysis Date = 04/04/15 Pct Recovery = 61% Analysis Date = 04/04/15 Pct Recovery = 61% Analysis Date = 03/30/15 Pct Recovery = 62% Analysis Date = 03/30/15 Pct Recovery = 62% Analysis Date = 03/25/15 Pct Recovery = 62% Analysis Date = 03/25/15 Pct Recovery = 62% Analysis Date = 03/21/15 Pct Recovery = 62% Analysis Date = 03/21/15 Pct Recovery = 62% Analysis Date = 03/16/15 Pct Recovery = 62% Analysis Date = 03/16/15 Pct Recovery = 62% Analysis Date = 03/11/15 Pct Recovery = 63% Analysis Date = 03/11/15 Pct Recovery = 63% Analysis Date = 03/06/15 Pct Recovery = 63% Analysis Date = 03/06/15 Pct Recovery = 63% Analysis Date = 03/01/15 Pct Recovery = 63% Analysis Date = 03/01/15 Pct Recovery = 63% Analysis Date = 02/24/15 Pct Recovery = 63% Analysis Date = 02/24/15 Pct Recovery = 63% Analysis Date = 02/19/15 Pct Recovery = 64% Analysis Date = 02/19/15 Pct Recovery = 64% Analysis Date = 02/14/15 Pct Recovery = 64% Analysis Date = 02/14/15 Pct Recovery = 64% Analysis Date = 02/09/15 Pct Recovery = 64% Analysis Date = 02/09/15 Pct Recovery = 64% Analysis Date = 02/05/15 Pct Recovery = 64% Analysis Date = 02/05/15 Pct Recovery = 64% Analysis Date = 01/31/15 Pct Recovery = 64% Analysis Date = 01/31/15 Pct Recovery = 64% Analysis Date = 01/26/15 Pct Recovery = 65% Analysis Date = 01/26/15 Pct Recovery = 65% Analysis Date = 01/21/15 Pct Recovery = 65% Analysis Date = 01/21/15 Pct Recovery = 65% Analysis Date = 01/16/15 Pct Recovery = 65% Analysis Date = 01/16/15 Pct Recovery = 65% Analysis Date = 01/11/15 Pct Recovery = 65% Analysis Date = 01/11/15 Pct Recovery = 65% Analysis Date = 01/06/15 Pct Recovery = 66% Analysis Date = 01/06/15 Pct Recovery = 66% Analysis Date = 01/01/15 Pct Recovery = 66% Analysis Date = 01/01/15 Pct Recovery = 66% Analysis Date = 12/27/14 Pct Recovery = 66% Analysis Date = 12/27/14 Pct Recovery = 66% Analysis Date = 12/23/14 Pct Recovery = 66% Analysis Date = 12/23/14 Pct Recovery = 66% Analysis Date = 12/18/14 Pct Recovery = 66% Analysis Date = 12/18/14 Pct Recovery = 66% Analysis Date = 12/13/14 Pct Recovery = 67% Analysis Date = 12/13/14 Pct Recovery = 67% Analysis Date = 12/08/14 Pct Recovery = 67% Analysis Date = 12/08/14 Pct Recovery = 67% Analysis Date = 12/03/14 Pct Recovery = 67% Analysis Date = 12/03/14 Pct Recovery = 67% Analysis Date = 11/28/14 Pct Recovery = 67% Analysis Date = 11/28/14 Pct Recovery = 67% Analysis Date = 11/23/14 Pct Recovery = 68% Analysis Date = 11/23/14 Pct Recovery = 68% Analysis Date = 11/18/14 Pct Recovery = 68% Analysis Date = 11/18/14 Pct Recovery = 68% Analysis Date = 11/13/14 Pct Recovery = 68% Analysis Date = 11/13/14 Pct Recovery = 68% Analysis Date = 11/09/14 Pct Recovery = 68% Analysis Date = 11/09/14 Pct Recovery = 68% Analysis Date = 11/04/14 Pct Recovery = 69% Analysis Date = 11/04/14 Pct Recovery = 69% Analysis Date = 10/30/14 Pct Recovery = 69% Analysis Date = 10/30/14 Pct Recovery = 69% Analysis Date = 10/25/14 Pct Recovery = 69% Analysis Date = 10/25/14 Pct Recovery = 69% Analysis Date = 10/20/14 Pct Recovery = 69% Analysis Date = 10/20/14 Pct Recovery = 69% Analysis Date = 10/15/14 Pct Recovery = 69% Analysis Date = 10/15/14 Pct Recovery = 69% Analysis Date = 10/10/14 Pct Recovery = 70% Analysis Date = 10/10/14 Pct Recovery = 70% Analysis Date = 10/05/14 Pct Recovery = 70% Analysis Date = 10/05/14 Pct Recovery = 70% Analysis Date = 09/30/14 Pct Recovery = 70% Analysis Date = 09/30/14 Pct Recovery = 70% Analysis Date = 09/26/14 Pct Recovery = 70% Analysis Date = 09/26/14 Pct Recovery = 70% Analysis Date = 09/21/14 Pct Recovery = 71% Analysis Date = 09/21/14 Pct Recovery = 71% Analysis Date = 09/16/14 Pct Recovery = 71% Analysis Date = 09/16/14 Pct Recovery = 71% Analysis Date = 09/11/14 Pct Recovery = 71% Analysis Date = 09/11/14 Pct Recovery = 71% Analysis Date = 09/06/14 Pct Recovery = 71% Analysis Date = 09/06/14 Pct Recovery = 71% Analysis Date = 09/01/14 Pct Recovery = 71% Analysis Date = 09/01/14 Pct Recovery = 71% Analysis Date = 08/27/14 Pct Recovery = 72% Analysis Date = 08/27/14 Pct Recovery = 72% Analysis Date = 08/22/14 Pct Recovery = 72% Analysis Date = 08/22/14 Pct Recovery = 72% Analysis Date = 08/17/14 Pct Recovery = 72% Analysis Date = 08/17/14 Pct Recovery = 72% Analysis Date = 08/13/14 Pct Recovery = 72% Analysis Date = 08/13/14 Pct Recovery = 72% Analysis Date = 08/08/14 Pct Recovery = 73% Analysis Date = 08/08/14 Pct Recovery = 73% Analysis Date = 08/03/14 Pct Recovery = 73% Analysis Date = 08/03/14 Pct Recovery = 73% Analysis Date = 07/29/14 Pct Recovery = 73% Analysis Date = 07/29/14 Pct Recovery = 73% Analysis Date = 07/24/14 Pct Recovery = 73% Analysis Date = 07/24/14 Pct Recovery = 73% Analysis Date = 07/19/14 Pct Recovery = 73% Analysis Date = 07/19/14 Pct Recovery = 73% Analysis Date = 07/14/14 Pct Recovery = 74% Analysis Date = 07/14/14 Pct Recovery = 74% Analysis Date = 07/09/14 Pct Recovery = 74% Analysis Date = 07/09/14 Pct Recovery = 74% Analysis Date = 07/04/14 Pct Recovery = 74% Analysis Date = 07/04/14 Pct Recovery = 74% Analysis Date = 06/30/14 Pct Recovery = 74% Analysis Date = 06/30/14 Pct Recovery = 74% Analysis Date = 06/25/14 Pct Recovery = 75% Analysis Date = 06/25/14 Pct Recovery = 75% Analysis Date = 06/20/14 Pct Recovery = 75% Analysis Date = 06/20/14 Pct Recovery = 75% Analysis Date = 06/15/14 Pct Recovery = 75% Analysis Date = 06/15/14 Pct Recovery = 75% Analysis Date = 06/10/14 Pct Recovery = 75% Analysis Date = 06/10/14 Pct Recovery = 75% Analysis Date = 06/05/14 Pct Recovery = 76% Analysis Date = 06/05/14 Pct Recovery = 76% Analysis Date = 05/31/14 Pct Recovery = 76% Analysis Date = 05/31/14 Pct Recovery = 76% Analysis Date = 05/26/14 Pct Recovery = 76% Analysis Date = 05/26/14 Pct Recovery = 76% Analysis Date = 05/21/14 Pct Recovery = 76% Analysis Date = 05/21/14 Pct Recovery = 76% Analysis Date = 05/17/14 Pct Recovery = 76% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
METHOTREXATE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 60 56% 18% 53% 18%
Total 60 56% 18% 53% 18%

Sample Statistics
METHOTREXATE

Characteristic N % % Basis
Plotted 60 78% Spiked
Estimated Values 52 68% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 2 3% Spiked
Spiked 77 .  
False Negatives 15 19% 15 out of 77
Not Spiked 38 .  
False Positives 0 0% 0 out of 38

BQS OBSP Determination:
METHYL-1H-BENZOTRIAZOLE
METHOD: 2440 , TESTIDCODE: 67514LCM56
Open Data Set

Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 113% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 108% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 92% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 88% Analysis Date = 01/17/16 SpikeMix = ERA 0406-15-09: 80 µl & ERA 0406-15-07A: 80 µl Pct Recovery = 73% Analysis Date = 11/24/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 78% Analysis Date = 10/01/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 89% Analysis Date = 11/05/15 SpikeMix = ERA 0406-15-08: 80 µl & Abs 052215: 80 µl Pct Recovery = 91% Analysis Date = 11/04/15 SpikeMix = Abs 052215: 80 µl & Abs 050115: 80 µl Pct Recovery = 93% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 89% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 87% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 85% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 82% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 83% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 79% Analysis Date = 09/24/16 SpikeMix = Crescent EN160610015: 80 µl & Abs 061416: 80 µl Pct Recovery = 79% Analysis Date = 09/24/16 SpikeMix = Abs 061416: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 78% Analysis Date = 05/07/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 111% Analysis Date = 03/11/15 SpikeMix = ERA 0318-14-02: 15 µl & Abs 041714: 15 µl Pct Recovery = 106% Analysis Date = 01/16/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 92% Analysis Date = 12/06/14 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 83% Analysis Date = 08/21/14 SpikeMix = ERA 0318-14-02: 60 µl & Abs 041714: 60 µl Pct Recovery = 79% Analysis Date = 07/12/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 78% Analysis Date = 06/11/14 SpikeMix = Abs 041614: 60 µl & Abs 041714: 60 µl Pct Recovery = 93% Analysis Date = 05/21/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 85% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-04: 15 µl & Abs 041814: 15 µl Pct Recovery = 85% Analysis Date = 12/06/14 SpikeMix = ERA 0318-14-02: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 78% Analysis Date = 10/25/14 SpikeMix = Abs 041614: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 85% Analysis Date = 10/11/14 SpikeMix = ERA 0318-14-02: 60 µl & ERA 0319-14-04: 60 µl Pct Recovery = 74% Analysis Date = 08/28/14 SpikeMix = ERA 0319-14-04: 60 µl & ERA 0319-14-05: 60 µl Pct Recovery = 65% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-08: 40 µl & ERA 0406-15-09: 40 µl Pct Recovery = 85% Analysis Date = 07/31/15 SpikeMix = ERA 0406-15-09: 40 µl & Abs 050115: 40 µl Pct Recovery = 101% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-08: 40 µl & Abs 052215: 40 µl Pct Recovery = 94% Analysis Date = 02/23/16 SpikeMix = Abs 052215: 40 µl & Abs 050115: 40 µl Pct Recovery = 86% Analysis Date = 09/10/15 SpikeMix = Abs 052215: 40 µl & ERA 0406-15-07A: 40 µl Pct Recovery = 96% Analysis Date = 07/31/15 SpikeMix = Abs 051315: 40 µl & Abs 052215: 40 µl Pct Recovery = 92% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 86% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 88% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 87% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 83% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 83% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 81% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 67% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 77% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 74% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 78% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 82% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 78% Analysis Date = 11/04/14 SpikeMix = Abs 041714: 8 µl & ERA 0319-14-05: 8 µl Pct Recovery = 83% Analysis Date = 04/30/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 104% Analysis Date = 04/10/15 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 86% Analysis Date = 02/10/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 84% Analysis Date = 12/07/14 SpikeMix = ERA 0318-14-02: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 77% Analysis Date = 10/11/14 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 75% Analysis Date = 10/10/14 SpikeMix = Abs 041714: 30 µl & Abs 041814: 30 µl Pct Recovery = 98% Analysis Date = 07/20/14 SpikeMix = ERA 0318-14-02: 30 µl & Abs 041714: 30 µl Pct Recovery = 73% Analysis Date = 06/28/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 86% Analysis Date = 05/17/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 87% Analysis Date = 09/12/14 SpikeMix = Abs 041614: 30 µl & ERA 0319-14-04: 30 µl Pct Recovery = 70% Analysis Date = 08/16/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 68% Analysis Date = 07/13/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 78% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 109% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 83% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-08: 20 µl & ERA 0406-15-09: 20 µl Pct Recovery = 78% Analysis Date = 11/24/15 SpikeMix = ERA 0406-15-09: 20 µl & Abs 050115: 20 µl Pct Recovery = 79% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-09: 20 µl Pct Recovery = 74% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 65% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 61% Analysis Date = 02/23/16 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 77% Analysis Date = 11/24/15 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 87% Analysis Date = 09/09/15 SpikeMix = ERA 0406-15-08: 20 µl & Abs 052215: 20 µl Pct Recovery = 104% Analysis Date = 08/27/15 SpikeMix = Abs 052215: 20 µl & Abs 050115: 20 µl Pct Recovery = 79% Analysis Date = 07/09/15 SpikeMix = Abs 050115: 20 µl & Abs 052215: 20 µl Pct Recovery = 82% Analysis Date = 06/26/15 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 89% Analysis Date = 04/09/16 SpikeMix = Abs 051315: 10 µl & ERA 0406-15-09: 10 µl Pct Recovery = 90% Analysis Date = 04/09/16 SpikeMix = Abs 051315: 10 µl & ERA 0406-15-09: 10 µl Pct Recovery = 99% Analysis Date = 01/18/17 Pct Recovery = 88% Analysis Date = 01/14/17 Pct Recovery = 88% Analysis Date = 01/14/17 Pct Recovery = 88% Analysis Date = 01/09/17 Pct Recovery = 88% Analysis Date = 01/09/17 Pct Recovery = 88% Analysis Date = 01/04/17 Pct Recovery = 88% Analysis Date = 01/04/17 Pct Recovery = 88% Analysis Date = 12/30/16 Pct Recovery = 87% Analysis Date = 12/30/16 Pct Recovery = 87% Analysis Date = 12/25/16 Pct Recovery = 87% Analysis Date = 12/25/16 Pct Recovery = 87% Analysis Date = 12/20/16 Pct Recovery = 87% Analysis Date = 12/20/16 Pct Recovery = 87% Analysis Date = 12/15/16 Pct Recovery = 87% Analysis Date = 12/15/16 Pct Recovery = 87% Analysis Date = 12/10/16 Pct Recovery = 87% Analysis Date = 12/10/16 Pct Recovery = 87% Analysis Date = 12/05/16 Pct Recovery = 87% Analysis Date = 12/05/16 Pct Recovery = 87% Analysis Date = 12/01/16 Pct Recovery = 87% Analysis Date = 12/01/16 Pct Recovery = 87% Analysis Date = 11/26/16 Pct Recovery = 86% Analysis Date = 11/26/16 Pct Recovery = 86% Analysis Date = 11/21/16 Pct Recovery = 86% Analysis Date = 11/21/16 Pct Recovery = 86% Analysis Date = 11/16/16 Pct Recovery = 86% Analysis Date = 11/16/16 Pct Recovery = 86% Analysis Date = 11/11/16 Pct Recovery = 86% Analysis Date = 11/11/16 Pct Recovery = 86% Analysis Date = 11/06/16 Pct Recovery = 86% Analysis Date = 11/06/16 Pct Recovery = 86% Analysis Date = 11/01/16 Pct Recovery = 86% Analysis Date = 11/01/16 Pct Recovery = 86% Analysis Date = 10/27/16 Pct Recovery = 86% Analysis Date = 10/27/16 Pct Recovery = 86% Analysis Date = 10/22/16 Pct Recovery = 85% Analysis Date = 10/22/16 Pct Recovery = 85% Analysis Date = 10/18/16 Pct Recovery = 85% Analysis Date = 10/18/16 Pct Recovery = 85% Analysis Date = 10/13/16 Pct Recovery = 85% Analysis Date = 10/13/16 Pct Recovery = 85% Analysis Date = 10/08/16 Pct Recovery = 85% Analysis Date = 10/08/16 Pct Recovery = 85% Analysis Date = 10/03/16 Pct Recovery = 85% Analysis Date = 10/03/16 Pct Recovery = 85% Analysis Date = 09/28/16 Pct Recovery = 85% Analysis Date = 09/28/16 Pct Recovery = 85% Analysis Date = 09/23/16 Pct Recovery = 85% Analysis Date = 09/23/16 Pct Recovery = 85% Analysis Date = 09/18/16 Pct Recovery = 85% Analysis Date = 09/18/16 Pct Recovery = 85% Analysis Date = 09/13/16 Pct Recovery = 85% Analysis Date = 09/13/16 Pct Recovery = 85% Analysis Date = 09/08/16 Pct Recovery = 84% Analysis Date = 09/08/16 Pct Recovery = 84% Analysis Date = 09/04/16 Pct Recovery = 84% Analysis Date = 09/04/16 Pct Recovery = 84% Analysis Date = 08/30/16 Pct Recovery = 84% Analysis Date = 08/30/16 Pct Recovery = 84% Analysis Date = 08/25/16 Pct Recovery = 84% Analysis Date = 08/25/16 Pct Recovery = 84% Analysis Date = 08/20/16 Pct Recovery = 84% Analysis Date = 08/20/16 Pct Recovery = 84% Analysis Date = 08/15/16 Pct Recovery = 84% Analysis Date = 08/15/16 Pct Recovery = 84% Analysis Date = 08/10/16 Pct Recovery = 84% Analysis Date = 08/10/16 Pct Recovery = 84% Analysis Date = 08/05/16 Pct Recovery = 84% Analysis Date = 08/05/16 Pct Recovery = 84% Analysis Date = 07/31/16 Pct Recovery = 84% Analysis Date = 07/31/16 Pct Recovery = 84% Analysis Date = 07/26/16 Pct Recovery = 84% Analysis Date = 07/26/16 Pct Recovery = 84% Analysis Date = 07/22/16 Pct Recovery = 84% Analysis Date = 07/22/16 Pct Recovery = 84% Analysis Date = 07/17/16 Pct Recovery = 84% Analysis Date = 07/17/16 Pct Recovery = 84% Analysis Date = 07/12/16 Pct Recovery = 84% Analysis Date = 07/12/16 Pct Recovery = 84% Analysis Date = 07/07/16 Pct Recovery = 84% Analysis Date = 07/07/16 Pct Recovery = 84% Analysis Date = 07/02/16 Pct Recovery = 84% Analysis Date = 07/02/16 Pct Recovery = 84% Analysis Date = 06/27/16 Pct Recovery = 84% Analysis Date = 06/27/16 Pct Recovery = 84% Analysis Date = 06/22/16 Pct Recovery = 84% Analysis Date = 06/22/16 Pct Recovery = 84% Analysis Date = 06/17/16 Pct Recovery = 84% Analysis Date = 06/17/16 Pct Recovery = 84% Analysis Date = 06/12/16 Pct Recovery = 84% Analysis Date = 06/12/16 Pct Recovery = 84% Analysis Date = 06/08/16 Pct Recovery = 84% Analysis Date = 06/08/16 Pct Recovery = 84% Analysis Date = 06/03/16 Pct Recovery = 84% Analysis Date = 06/03/16 Pct Recovery = 84% Analysis Date = 05/29/16 Pct Recovery = 83% Analysis Date = 05/29/16 Pct Recovery = 83% Analysis Date = 05/24/16 Pct Recovery = 83% Analysis Date = 05/24/16 Pct Recovery = 83% Analysis Date = 05/19/16 Pct Recovery = 83% Analysis Date = 05/19/16 Pct Recovery = 83% Analysis Date = 05/14/16 Pct Recovery = 83% Analysis Date = 05/14/16 Pct Recovery = 83% Analysis Date = 05/09/16 Pct Recovery = 83% Analysis Date = 05/09/16 Pct Recovery = 83% Analysis Date = 05/04/16 Pct Recovery = 83% Analysis Date = 05/04/16 Pct Recovery = 83% Analysis Date = 04/29/16 Pct Recovery = 83% Analysis Date = 04/29/16 Pct Recovery = 83% Analysis Date = 04/25/16 Pct Recovery = 83% Analysis Date = 04/25/16 Pct Recovery = 83% Analysis Date = 04/20/16 Pct Recovery = 83% Analysis Date = 04/20/16 Pct Recovery = 83% Analysis Date = 04/15/16 Pct Recovery = 83% Analysis Date = 04/15/16 Pct Recovery = 83% Analysis Date = 04/10/16 Pct Recovery = 83% Analysis Date = 04/10/16 Pct Recovery = 83% Analysis Date = 04/05/16 Pct Recovery = 83% Analysis Date = 04/05/16 Pct Recovery = 83% Analysis Date = 03/31/16 Pct Recovery = 83% Analysis Date = 03/31/16 Pct Recovery = 83% Analysis Date = 03/26/16 Pct Recovery = 83% Analysis Date = 03/26/16 Pct Recovery = 83% Analysis Date = 03/21/16 Pct Recovery = 84% Analysis Date = 03/21/16 Pct Recovery = 84% Analysis Date = 03/16/16 Pct Recovery = 84% Analysis Date = 03/16/16 Pct Recovery = 84% Analysis Date = 03/12/16 Pct Recovery = 84% Analysis Date = 03/12/16 Pct Recovery = 84% Analysis Date = 03/07/16 Pct Recovery = 84% Analysis Date = 03/07/16 Pct Recovery = 84% Analysis Date = 03/02/16 Pct Recovery = 84% Analysis Date = 03/02/16 Pct Recovery = 84% Analysis Date = 02/26/16 Pct Recovery = 84% Analysis Date = 02/26/16 Pct Recovery = 84% Analysis Date = 02/21/16 Pct Recovery = 84% Analysis Date = 02/21/16 Pct Recovery = 84% Analysis Date = 02/16/16 Pct Recovery = 84% Analysis Date = 02/16/16 Pct Recovery = 84% Analysis Date = 02/11/16 Pct Recovery = 84% Analysis Date = 02/11/16 Pct Recovery = 84% Analysis Date = 02/06/16 Pct Recovery = 85% Analysis Date = 02/06/16 Pct Recovery = 85% Analysis Date = 02/01/16 Pct Recovery = 85% Analysis Date = 02/01/16 Pct Recovery = 85% Analysis Date = 01/28/16 Pct Recovery = 85% Analysis Date = 01/28/16 Pct Recovery = 85% Analysis Date = 01/23/16 Pct Recovery = 85% Analysis Date = 01/23/16 Pct Recovery = 85% Analysis Date = 01/18/16 Pct Recovery = 85% Analysis Date = 01/18/16 Pct Recovery = 85% Analysis Date = 01/13/16 Pct Recovery = 85% Analysis Date = 01/13/16 Pct Recovery = 85% Analysis Date = 01/08/16 Pct Recovery = 85% Analysis Date = 01/08/16 Pct Recovery = 85% Analysis Date = 01/03/16 Pct Recovery = 85% Analysis Date = 01/03/16 Pct Recovery = 85% Analysis Date = 12/29/15 Pct Recovery = 86% Analysis Date = 12/29/15 Pct Recovery = 86% Analysis Date = 12/24/15 Pct Recovery = 86% Analysis Date = 12/24/15 Pct Recovery = 86% Analysis Date = 12/19/15 Pct Recovery = 86% Analysis Date = 12/19/15 Pct Recovery = 86% Analysis Date = 12/15/15 Pct Recovery = 86% Analysis Date = 12/15/15 Pct Recovery = 86% Analysis Date = 12/10/15 Pct Recovery = 86% Analysis Date = 12/10/15 Pct Recovery = 86% Analysis Date = 12/05/15 Pct Recovery = 86% Analysis Date = 12/05/15 Pct Recovery = 86% Analysis Date = 11/30/15 Pct Recovery = 87% Analysis Date = 11/30/15 Pct Recovery = 87% Analysis Date = 11/25/15 Pct Recovery = 87% Analysis Date = 11/25/15 Pct Recovery = 87% Analysis Date = 11/20/15 Pct Recovery = 87% Analysis Date = 11/20/15 Pct Recovery = 87% Analysis Date = 11/15/15 Pct Recovery = 87% Analysis Date = 11/15/15 Pct Recovery = 87% Analysis Date = 11/10/15 Pct Recovery = 87% Analysis Date = 11/10/15 Pct Recovery = 87% Analysis Date = 11/05/15 Pct Recovery = 87% Analysis Date = 11/05/15 Pct Recovery = 87% Analysis Date = 11/01/15 Pct Recovery = 88% Analysis Date = 11/01/15 Pct Recovery = 88% Analysis Date = 10/27/15 Pct Recovery = 88% Analysis Date = 10/27/15 Pct Recovery = 88% Analysis Date = 10/22/15 Pct Recovery = 88% Analysis Date = 10/22/15 Pct Recovery = 88% Analysis Date = 10/17/15 Pct Recovery = 88% Analysis Date = 10/17/15 Pct Recovery = 88% Analysis Date = 10/12/15 Pct Recovery = 88% Analysis Date = 10/12/15 Pct Recovery = 88% Analysis Date = 10/07/15 Pct Recovery = 88% Analysis Date = 10/07/15 Pct Recovery = 88% Analysis Date = 10/02/15 Pct Recovery = 88% Analysis Date = 10/02/15 Pct Recovery = 88% Analysis Date = 09/27/15 Pct Recovery = 88% Analysis Date = 09/27/15 Pct Recovery = 88% Analysis Date = 09/22/15 Pct Recovery = 88% Analysis Date = 09/22/15 Pct Recovery = 88% Analysis Date = 09/17/15 Pct Recovery = 88% Analysis Date = 09/17/15 Pct Recovery = 88% Analysis Date = 09/13/15 Pct Recovery = 88% Analysis Date = 09/13/15 Pct Recovery = 88% Analysis Date = 09/08/15 Pct Recovery = 88% Analysis Date = 09/08/15 Pct Recovery = 88% Analysis Date = 09/03/15 Pct Recovery = 88% Analysis Date = 09/03/15 Pct Recovery = 88% Analysis Date = 08/29/15 Pct Recovery = 88% Analysis Date = 08/29/15 Pct Recovery = 88% Analysis Date = 08/24/15 Pct Recovery = 89% Analysis Date = 08/24/15 Pct Recovery = 89% Analysis Date = 08/19/15 Pct Recovery = 89% Analysis Date = 08/19/15 Pct Recovery = 89% Analysis Date = 08/14/15 Pct Recovery = 89% Analysis Date = 08/14/15 Pct Recovery = 89% Analysis Date = 08/09/15 Pct Recovery = 89% Analysis Date = 08/09/15 Pct Recovery = 89% Analysis Date = 08/04/15 Pct Recovery = 89% Analysis Date = 08/04/15 Pct Recovery = 89% Analysis Date = 07/31/15 Pct Recovery = 89% Analysis Date = 07/31/15 Pct Recovery = 89% Analysis Date = 07/26/15 Pct Recovery = 89% Analysis Date = 07/26/15 Pct Recovery = 89% Analysis Date = 07/21/15 Pct Recovery = 89% Analysis Date = 07/21/15 Pct Recovery = 89% Analysis Date = 07/16/15 Pct Recovery = 89% Analysis Date = 07/16/15 Pct Recovery = 89% Analysis Date = 07/11/15 Pct Recovery = 89% Analysis Date = 07/11/15 Pct Recovery = 89% Analysis Date = 07/06/15 Pct Recovery = 89% Analysis Date = 07/06/15 Pct Recovery = 89% Analysis Date = 07/01/15 Pct Recovery = 89% Analysis Date = 07/01/15 Pct Recovery = 89% Analysis Date = 06/26/15 Pct Recovery = 89% Analysis Date = 06/26/15 Pct Recovery = 89% Analysis Date = 06/21/15 Pct Recovery = 88% Analysis Date = 06/21/15 Pct Recovery = 88% Analysis Date = 06/17/15 Pct Recovery = 88% Analysis Date = 06/17/15 Pct Recovery = 88% Analysis Date = 06/12/15 Pct Recovery = 88% Analysis Date = 06/12/15 Pct Recovery = 88% Analysis Date = 06/07/15 Pct Recovery = 88% Analysis Date = 06/07/15 Pct Recovery = 88% Analysis Date = 06/02/15 Pct Recovery = 88% Analysis Date = 06/02/15 Pct Recovery = 88% Analysis Date = 05/28/15 Pct Recovery = 88% Analysis Date = 05/28/15 Pct Recovery = 88% Analysis Date = 05/23/15 Pct Recovery = 88% Analysis Date = 05/23/15 Pct Recovery = 88% Analysis Date = 05/18/15 Pct Recovery = 88% Analysis Date = 05/18/15 Pct Recovery = 88% Analysis Date = 05/13/15 Pct Recovery = 88% Analysis Date = 05/13/15 Pct Recovery = 88% Analysis Date = 05/08/15 Pct Recovery = 88% Analysis Date = 05/08/15 Pct Recovery = 88% Analysis Date = 05/04/15 Pct Recovery = 88% Analysis Date = 05/04/15 Pct Recovery = 88% Analysis Date = 04/29/15 Pct Recovery = 88% Analysis Date = 04/29/15 Pct Recovery = 88% Analysis Date = 04/24/15 Pct Recovery = 88% Analysis Date = 04/24/15 Pct Recovery = 88% Analysis Date = 04/19/15 Pct Recovery = 88% Analysis Date = 04/19/15 Pct Recovery = 88% Analysis Date = 04/14/15 Pct Recovery = 88% Analysis Date = 04/14/15 Pct Recovery = 88% Analysis Date = 04/09/15 Pct Recovery = 88% Analysis Date = 04/09/15 Pct Recovery = 88% Analysis Date = 04/04/15 Pct Recovery = 88% Analysis Date = 04/04/15 Pct Recovery = 88% Analysis Date = 03/30/15 Pct Recovery = 87% Analysis Date = 03/30/15 Pct Recovery = 87% Analysis Date = 03/25/15 Pct Recovery = 87% Analysis Date = 03/25/15 Pct Recovery = 87% Analysis Date = 03/21/15 Pct Recovery = 87% Analysis Date = 03/21/15 Pct Recovery = 87% Analysis Date = 03/16/15 Pct Recovery = 87% Analysis Date = 03/16/15 Pct Recovery = 87% Analysis Date = 03/11/15 Pct Recovery = 87% Analysis Date = 03/11/15 Pct Recovery = 87% Analysis Date = 03/06/15 Pct Recovery = 87% Analysis Date = 03/06/15 Pct Recovery = 87% Analysis Date = 03/01/15 Pct Recovery = 87% Analysis Date = 03/01/15 Pct Recovery = 87% Analysis Date = 02/24/15 Pct Recovery = 86% Analysis Date = 02/24/15 Pct Recovery = 86% Analysis Date = 02/19/15 Pct Recovery = 86% Analysis Date = 02/19/15 Pct Recovery = 86% Analysis Date = 02/14/15 Pct Recovery = 86% Analysis Date = 02/14/15 Pct Recovery = 86% Analysis Date = 02/09/15 Pct Recovery = 86% Analysis Date = 02/09/15 Pct Recovery = 86% Analysis Date = 02/05/15 Pct Recovery = 86% Analysis Date = 02/05/15 Pct Recovery = 86% Analysis Date = 01/31/15 Pct Recovery = 86% Analysis Date = 01/31/15 Pct Recovery = 86% Analysis Date = 01/26/15 Pct Recovery = 86% Analysis Date = 01/26/15 Pct Recovery = 86% Analysis Date = 01/21/15 Pct Recovery = 85% Analysis Date = 01/21/15 Pct Recovery = 85% Analysis Date = 01/16/15 Pct Recovery = 85% Analysis Date = 01/16/15 Pct Recovery = 85% Analysis Date = 01/11/15 Pct Recovery = 85% Analysis Date = 01/11/15 Pct Recovery = 85% Analysis Date = 01/06/15 Pct Recovery = 85% Analysis Date = 01/06/15 Pct Recovery = 85% Analysis Date = 01/01/15 Pct Recovery = 85% Analysis Date = 01/01/15 Pct Recovery = 85% Analysis Date = 12/27/14 Pct Recovery = 85% Analysis Date = 12/27/14 Pct Recovery = 85% Analysis Date = 12/23/14 Pct Recovery = 85% Analysis Date = 12/23/14 Pct Recovery = 85% Analysis Date = 12/18/14 Pct Recovery = 84% Analysis Date = 12/18/14 Pct Recovery = 84% Analysis Date = 12/13/14 Pct Recovery = 84% Analysis Date = 12/13/14 Pct Recovery = 84% Analysis Date = 12/08/14 Pct Recovery = 84% Analysis Date = 12/08/14 Pct Recovery = 84% Analysis Date = 12/03/14 Pct Recovery = 84% Analysis Date = 12/03/14 Pct Recovery = 84% Analysis Date = 11/28/14 Pct Recovery = 84% Analysis Date = 11/28/14 Pct Recovery = 84% Analysis Date = 11/23/14 Pct Recovery = 84% Analysis Date = 11/23/14 Pct Recovery = 84% Analysis Date = 11/18/14 Pct Recovery = 84% Analysis Date = 11/18/14 Pct Recovery = 84% Analysis Date = 11/13/14 Pct Recovery = 83% Analysis Date = 11/13/14 Pct Recovery = 83% Analysis Date = 11/09/14 Pct Recovery = 83% Analysis Date = 11/09/14 Pct Recovery = 83% Analysis Date = 11/04/14 Pct Recovery = 83% Analysis Date = 11/04/14 Pct Recovery = 83% Analysis Date = 10/30/14 Pct Recovery = 83% Analysis Date = 10/30/14 Pct Recovery = 83% Analysis Date = 10/25/14 Pct Recovery = 83% Analysis Date = 10/25/14 Pct Recovery = 83% Analysis Date = 10/20/14 Pct Recovery = 83% Analysis Date = 10/20/14 Pct Recovery = 83% Analysis Date = 10/15/14 Pct Recovery = 83% Analysis Date = 10/15/14 Pct Recovery = 83% Analysis Date = 10/10/14 Pct Recovery = 82% Analysis Date = 10/10/14 Pct Recovery = 82% Analysis Date = 10/05/14 Pct Recovery = 82% Analysis Date = 10/05/14 Pct Recovery = 82% Analysis Date = 09/30/14 Pct Recovery = 82% Analysis Date = 09/30/14 Pct Recovery = 82% Analysis Date = 09/26/14 Pct Recovery = 82% Analysis Date = 09/26/14 Pct Recovery = 82% Analysis Date = 09/21/14 Pct Recovery = 82% Analysis Date = 09/21/14 Pct Recovery = 82% Analysis Date = 09/16/14 Pct Recovery = 82% Analysis Date = 09/16/14 Pct Recovery = 82% Analysis Date = 09/11/14 Pct Recovery = 82% Analysis Date = 09/11/14 Pct Recovery = 82% Analysis Date = 09/06/14 Pct Recovery = 81% Analysis Date = 09/06/14 Pct Recovery = 81% Analysis Date = 09/01/14 Pct Recovery = 81% Analysis Date = 09/01/14 Pct Recovery = 81% Analysis Date = 08/27/14 Pct Recovery = 81% Analysis Date = 08/27/14 Pct Recovery = 81% Analysis Date = 08/22/14 Pct Recovery = 81% Analysis Date = 08/22/14 Pct Recovery = 81% Analysis Date = 08/17/14 Pct Recovery = 81% Analysis Date = 08/17/14 Pct Recovery = 81% Analysis Date = 08/13/14 Pct Recovery = 81% Analysis Date = 08/13/14 Pct Recovery = 81% Analysis Date = 08/08/14 Pct Recovery = 80% Analysis Date = 08/08/14 Pct Recovery = 80% Analysis Date = 08/03/14 Pct Recovery = 80% Analysis Date = 08/03/14 Pct Recovery = 80% Analysis Date = 07/29/14 Pct Recovery = 80% Analysis Date = 07/29/14 Pct Recovery = 80% Analysis Date = 07/24/14 Pct Recovery = 80% Analysis Date = 07/24/14 Pct Recovery = 80% Analysis Date = 07/19/14 Pct Recovery = 80% Analysis Date = 07/19/14 Pct Recovery = 80% Analysis Date = 07/14/14 Pct Recovery = 80% Analysis Date = 07/14/14 Pct Recovery = 80% Analysis Date = 07/09/14 Pct Recovery = 80% Analysis Date = 07/09/14 Pct Recovery = 80% Analysis Date = 07/04/14 Pct Recovery = 79% Analysis Date = 07/04/14 Pct Recovery = 79% Analysis Date = 06/30/14 Pct Recovery = 79% Analysis Date = 06/30/14 Pct Recovery = 79% Analysis Date = 06/25/14 Pct Recovery = 79% Analysis Date = 06/25/14 Pct Recovery = 79% Analysis Date = 06/20/14 Pct Recovery = 79% Analysis Date = 06/20/14 Pct Recovery = 79% Analysis Date = 06/15/14 Pct Recovery = 79% Analysis Date = 06/15/14 Pct Recovery = 79% Analysis Date = 06/10/14 Pct Recovery = 79% Analysis Date = 06/10/14 Pct Recovery = 79% Analysis Date = 06/05/14 Pct Recovery = 78% Analysis Date = 06/05/14 Pct Recovery = 78% Analysis Date = 05/31/14 Pct Recovery = 78% Analysis Date = 05/31/14 Pct Recovery = 78% Analysis Date = 05/26/14 Pct Recovery = 78% Analysis Date = 05/26/14 Pct Recovery = 78% Analysis Date = 05/21/14 Pct Recovery = 78% Analysis Date = 05/21/14 Pct Recovery = 78% Analysis Date = 05/17/14 Pct Recovery = 78% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
METHYL-1H-BENZOTRIAZOLE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 2 95% 6% 95% 7%
>= Reporting Level 74 85% 11% 83% 8%
Total 76 85% 11% 84% 9%

Sample Statistics
METHYL-1H-BENZOTRIAZOLE

Characteristic N % % Basis
Plotted 76 100% Spiked
Estimated Values 13 17% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 76 .  
False Negatives 0 0% 0 out of 76
Not Spiked 39 .  
False Positives 0 0% 0 out of 39

BQS OBSP Determination:
METOPROLOL
METHOD: 2440 , TESTIDCODE: 67523LCM56
Open Data Set

Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 36% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 35% Analysis Date = 11/24/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 39% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 80 µl & Abs 051315: 80 µl Pct Recovery = 40% Analysis Date = 10/01/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 36% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 80 µl & ERA 0406-15-08: 80 µl Pct Recovery = 39% Analysis Date = 11/05/15 SpikeMix = ERA 0406-15-08: 80 µl & Abs 052215: 80 µl Pct Recovery = 37% Analysis Date = 11/18/16 SpikeMix = ERA 04281604: 80 µl & ERA 04281603: 80 µl Pct Recovery = 36% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & ERA 04281604: 80 µl Pct Recovery = 34% Analysis Date = 09/24/16 SpikeMix = Crescent EN160610015: 80 µl & Abs 061416: 80 µl Pct Recovery = 35% Analysis Date = 09/24/16 SpikeMix = Abs 061416: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 35% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 44% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 42% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 44% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 42% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 44% Analysis Date = 12/07/14 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 36% Analysis Date = 10/25/14 SpikeMix = Abs 041614: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 35% Analysis Date = 06/22/14 SpikeMix = Abs 041814: 60 µl & Abs 041614: 60 µl Pct Recovery = 43% Analysis Date = 06/11/14 SpikeMix = Abs 041614: 60 µl & Abs 041714: 60 µl Pct Recovery = 34% Analysis Date = 04/29/15 SpikeMix = ERA 0319-14-05: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 46% Analysis Date = 02/06/15 SpikeMix = Abs 041814: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 41% Analysis Date = 12/06/14 SpikeMix = ERA 0318-14-02: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 32% Analysis Date = 10/11/14 SpikeMix = ERA 0318-14-02: 60 µl & ERA 0319-14-04: 60 µl Pct Recovery = 30% Analysis Date = 08/21/14 SpikeMix = ERA 0318-14-02: 60 µl & Abs 041714: 60 µl Pct Recovery = 31% Analysis Date = 07/26/14 SpikeMix = ERA 0319-14-05: 60 µl & ERA 0318-14-02: 60 µl Pct Recovery = 37% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 36% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 31% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-07A: 40 µl & Abs 051315: 40 µl Pct Recovery = 34% Analysis Date = 07/31/15 SpikeMix = Abs 051315: 40 µl & Abs 052215: 40 µl Pct Recovery = 30% Analysis Date = 07/30/15 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 37% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-08: 40 µl & Abs 052215: 40 µl Pct Recovery = 37% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 35% Analysis Date = 11/04/15 SpikeMix = ERA 0406-15-07A: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 35% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-08: 40 µl & ERA 0406-15-09: 40 µl Pct Recovery = 38% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 46% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 48% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 28% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 26% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 41% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 38% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 29% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 29% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 34% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 34% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 26% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 29% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 29% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 30% Analysis Date = 04/30/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 39% Analysis Date = 02/10/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 42% Analysis Date = 10/24/14 SpikeMix = ERA 0319-14-05: 8 µl & Abs 041614: 8 µl Pct Recovery = 39% Analysis Date = 12/07/14 SpikeMix = ERA 0318-14-02: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 34% Analysis Date = 11/04/14 SpikeMix = Abs 041814: 8 µl & ERA 0318-14-02: 8 µl Pct Recovery = 35% Analysis Date = 09/12/14 SpikeMix = Abs 041614: 30 µl & ERA 0319-14-04: 30 µl Pct Recovery = 30% Analysis Date = 07/13/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 29% Analysis Date = 06/28/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 32% Analysis Date = 05/30/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 36% Analysis Date = 05/17/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 35% Analysis Date = 10/10/14 SpikeMix = Abs 041814: 30 µl & ERA 0318-14-02: 30 µl Pct Recovery = 29% Analysis Date = 08/30/14 SpikeMix = ERA 0318-14-02: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 36% Analysis Date = 07/20/14 SpikeMix = ERA 0318-14-02: 30 µl & Abs 041714: 30 µl Pct Recovery = 30% Analysis Date = 02/23/16 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 37% Analysis Date = 08/11/15 SpikeMix = Abs 050115: 20 µl & Abs 051315: 20 µl Pct Recovery = 25% Analysis Date = 06/26/15 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 37% Analysis Date = 04/27/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 47% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 33% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-08: 20 µl & ERA 0406-15-09: 20 µl Pct Recovery = 34% Analysis Date = 11/25/15 SpikeMix = Abs 050115: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 36% Analysis Date = 09/15/15 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 35% Analysis Date = 09/09/15 SpikeMix = ERA 0406-15-08: 20 µl & Abs 052215: 20 µl Pct Recovery = 37% Analysis Date = 04/09/16 SpikeMix = Abs 051315: 10 µl & ERA 0406-15-09: 10 µl Pct Recovery = 29% Analysis Date = 04/09/16 SpikeMix = Abs 051315: 10 µl & ERA 0406-15-09: 10 µl Pct Recovery = 35% Analysis Date = 01/04/17 Pct Recovery = 36% Analysis Date = 12/31/16 Pct Recovery = 36% Analysis Date = 12/31/16 Pct Recovery = 36% Analysis Date = 12/26/16 Pct Recovery = 36% Analysis Date = 12/26/16 Pct Recovery = 36% Analysis Date = 12/21/16 Pct Recovery = 36% Analysis Date = 12/21/16 Pct Recovery = 36% Analysis Date = 12/16/16 Pct Recovery = 36% Analysis Date = 12/16/16 Pct Recovery = 36% Analysis Date = 12/11/16 Pct Recovery = 36% Analysis Date = 12/11/16 Pct Recovery = 36% Analysis Date = 12/07/16 Pct Recovery = 36% Analysis Date = 12/07/16 Pct Recovery = 36% Analysis Date = 12/02/16 Pct Recovery = 36% Analysis Date = 12/02/16 Pct Recovery = 36% Analysis Date = 11/27/16 Pct Recovery = 36% Analysis Date = 11/27/16 Pct Recovery = 36% Analysis Date = 11/22/16 Pct Recovery = 36% Analysis Date = 11/22/16 Pct Recovery = 36% Analysis Date = 11/17/16 Pct Recovery = 36% Analysis Date = 11/17/16 Pct Recovery = 36% Analysis Date = 11/12/16 Pct Recovery = 35% Analysis Date = 11/12/16 Pct Recovery = 35% Analysis Date = 11/08/16 Pct Recovery = 35% Analysis Date = 11/08/16 Pct Recovery = 35% Analysis Date = 11/03/16 Pct Recovery = 35% Analysis Date = 11/03/16 Pct Recovery = 35% Analysis Date = 10/29/16 Pct Recovery = 35% Analysis Date = 10/29/16 Pct Recovery = 35% Analysis Date = 10/24/16 Pct Recovery = 35% Analysis Date = 10/24/16 Pct Recovery = 35% Analysis Date = 10/19/16 Pct Recovery = 35% Analysis Date = 10/19/16 Pct Recovery = 35% Analysis Date = 10/15/16 Pct Recovery = 35% Analysis Date = 10/15/16 Pct Recovery = 35% Analysis Date = 10/10/16 Pct Recovery = 35% Analysis Date = 10/10/16 Pct Recovery = 35% Analysis Date = 10/05/16 Pct Recovery = 35% Analysis Date = 10/05/16 Pct Recovery = 35% Analysis Date = 09/30/16 Pct Recovery = 35% Analysis Date = 09/30/16 Pct Recovery = 35% Analysis Date = 09/25/16 Pct Recovery = 35% Analysis Date = 09/25/16 Pct Recovery = 35% Analysis Date = 09/20/16 Pct Recovery = 35% Analysis Date = 09/20/16 Pct Recovery = 35% Analysis Date = 09/16/16 Pct Recovery = 35% Analysis Date = 09/16/16 Pct Recovery = 35% Analysis Date = 09/11/16 Pct Recovery = 35% Analysis Date = 09/11/16 Pct Recovery = 35% Analysis Date = 09/06/16 Pct Recovery = 35% Analysis Date = 09/06/16 Pct Recovery = 35% Analysis Date = 09/01/16 Pct Recovery = 35% Analysis Date = 09/01/16 Pct Recovery = 35% Analysis Date = 08/27/16 Pct Recovery = 35% Analysis Date = 08/27/16 Pct Recovery = 35% Analysis Date = 08/23/16 Pct Recovery = 35% Analysis Date = 08/23/16 Pct Recovery = 35% Analysis Date = 08/18/16 Pct Recovery = 35% Analysis Date = 08/18/16 Pct Recovery = 35% Analysis Date = 08/13/16 Pct Recovery = 35% Analysis Date = 08/13/16 Pct Recovery = 35% Analysis Date = 08/08/16 Pct Recovery = 35% Analysis Date = 08/08/16 Pct Recovery = 35% Analysis Date = 08/03/16 Pct Recovery = 35% Analysis Date = 08/03/16 Pct Recovery = 35% Analysis Date = 07/29/16 Pct Recovery = 35% Analysis Date = 07/29/16 Pct Recovery = 35% Analysis Date = 07/25/16 Pct Recovery = 35% Analysis Date = 07/25/16 Pct Recovery = 35% Analysis Date = 07/20/16 Pct Recovery = 35% Analysis Date = 07/20/16 Pct Recovery = 35% Analysis Date = 07/15/16 Pct Recovery = 35% Analysis Date = 07/15/16 Pct Recovery = 35% Analysis Date = 07/10/16 Pct Recovery = 35% Analysis Date = 07/10/16 Pct Recovery = 35% Analysis Date = 07/05/16 Pct Recovery = 35% Analysis Date = 07/05/16 Pct Recovery = 35% Analysis Date = 07/01/16 Pct Recovery = 36% Analysis Date = 07/01/16 Pct Recovery = 36% Analysis Date = 06/26/16 Pct Recovery = 36% Analysis Date = 06/26/16 Pct Recovery = 36% Analysis Date = 06/21/16 Pct Recovery = 36% Analysis Date = 06/21/16 Pct Recovery = 36% Analysis Date = 06/16/16 Pct Recovery = 36% Analysis Date = 06/16/16 Pct Recovery = 36% Analysis Date = 06/11/16 Pct Recovery = 36% Analysis Date = 06/11/16 Pct Recovery = 36% Analysis Date = 06/06/16 Pct Recovery = 36% Analysis Date = 06/06/16 Pct Recovery = 36% Analysis Date = 06/02/16 Pct Recovery = 36% Analysis Date = 06/02/16 Pct Recovery = 36% Analysis Date = 05/28/16 Pct Recovery = 36% Analysis Date = 05/28/16 Pct Recovery = 36% Analysis Date = 05/23/16 Pct Recovery = 36% Analysis Date = 05/23/16 Pct Recovery = 36% Analysis Date = 05/18/16 Pct Recovery = 36% Analysis Date = 05/18/16 Pct Recovery = 36% Analysis Date = 05/13/16 Pct Recovery = 36% Analysis Date = 05/13/16 Pct Recovery = 36% Analysis Date = 05/08/16 Pct Recovery = 36% Analysis Date = 05/08/16 Pct Recovery = 36% Analysis Date = 05/04/16 Pct Recovery = 36% Analysis Date = 05/04/16 Pct Recovery = 36% Analysis Date = 04/29/16 Pct Recovery = 36% Analysis Date = 04/29/16 Pct Recovery = 36% Analysis Date = 04/24/16 Pct Recovery = 36% Analysis Date = 04/24/16 Pct Recovery = 36% Analysis Date = 04/19/16 Pct Recovery = 36% Analysis Date = 04/19/16 Pct Recovery = 36% Analysis Date = 04/14/16 Pct Recovery = 36% Analysis Date = 04/14/16 Pct Recovery = 36% Analysis Date = 04/10/16 Pct Recovery = 36% Analysis Date = 04/10/16 Pct Recovery = 36% Analysis Date = 04/05/16 Pct Recovery = 36% Analysis Date = 04/05/16 Pct Recovery = 36% Analysis Date = 03/31/16 Pct Recovery = 36% Analysis Date = 03/31/16 Pct Recovery = 36% Analysis Date = 03/26/16 Pct Recovery = 36% Analysis Date = 03/26/16 Pct Recovery = 36% Analysis Date = 03/21/16 Pct Recovery = 36% Analysis Date = 03/21/16 Pct Recovery = 36% Analysis Date = 03/16/16 Pct Recovery = 36% Analysis Date = 03/16/16 Pct Recovery = 36% Analysis Date = 03/12/16 Pct Recovery = 36% Analysis Date = 03/12/16 Pct Recovery = 36% Analysis Date = 03/07/16 Pct Recovery = 36% Analysis Date = 03/07/16 Pct Recovery = 36% Analysis Date = 03/02/16 Pct Recovery = 36% Analysis Date = 03/02/16 Pct Recovery = 36% Analysis Date = 02/26/16 Pct Recovery = 36% Analysis Date = 02/26/16 Pct Recovery = 36% Analysis Date = 02/21/16 Pct Recovery = 36% Analysis Date = 02/21/16 Pct Recovery = 36% Analysis Date = 02/17/16 Pct Recovery = 36% Analysis Date = 02/17/16 Pct Recovery = 36% Analysis Date = 02/12/16 Pct Recovery = 36% Analysis Date = 02/12/16 Pct Recovery = 36% Analysis Date = 02/07/16 Pct Recovery = 36% Analysis Date = 02/07/16 Pct Recovery = 36% Analysis Date = 02/02/16 Pct Recovery = 36% Analysis Date = 02/02/16 Pct Recovery = 36% Analysis Date = 01/28/16 Pct Recovery = 36% Analysis Date = 01/28/16 Pct Recovery = 36% Analysis Date = 01/23/16 Pct Recovery = 36% Analysis Date = 01/23/16 Pct Recovery = 36% Analysis Date = 01/19/16 Pct Recovery = 36% Analysis Date = 01/19/16 Pct Recovery = 36% Analysis Date = 01/14/16 Pct Recovery = 36% Analysis Date = 01/14/16 Pct Recovery = 36% Analysis Date = 01/09/16 Pct Recovery = 36% Analysis Date = 01/09/16 Pct Recovery = 36% Analysis Date = 01/04/16 Pct Recovery = 36% Analysis Date = 01/04/16 Pct Recovery = 36% Analysis Date = 12/30/15 Pct Recovery = 36% Analysis Date = 12/30/15 Pct Recovery = 36% Analysis Date = 12/26/15 Pct Recovery = 36% Analysis Date = 12/26/15 Pct Recovery = 36% Analysis Date = 12/21/15 Pct Recovery = 36% Analysis Date = 12/21/15 Pct Recovery = 36% Analysis Date = 12/16/15 Pct Recovery = 36% Analysis Date = 12/16/15 Pct Recovery = 36% Analysis Date = 12/11/15 Pct Recovery = 36% Analysis Date = 12/11/15 Pct Recovery = 36% Analysis Date = 12/06/15 Pct Recovery = 36% Analysis Date = 12/06/15 Pct Recovery = 36% Analysis Date = 12/01/15 Pct Recovery = 36% Analysis Date = 12/01/15 Pct Recovery = 36% Analysis Date = 11/27/15 Pct Recovery = 36% Analysis Date = 11/27/15 Pct Recovery = 36% Analysis Date = 11/22/15 Pct Recovery = 36% Analysis Date = 11/22/15 Pct Recovery = 36% Analysis Date = 11/17/15 Pct Recovery = 36% Analysis Date = 11/17/15 Pct Recovery = 36% Analysis Date = 11/12/15 Pct Recovery = 36% Analysis Date = 11/12/15 Pct Recovery = 36% Analysis Date = 11/07/15 Pct Recovery = 36% Analysis Date = 11/07/15 Pct Recovery = 36% Analysis Date = 11/03/15 Pct Recovery = 36% Analysis Date = 11/03/15 Pct Recovery = 36% Analysis Date = 10/29/15 Pct Recovery = 36% Analysis Date = 10/29/15 Pct Recovery = 36% Analysis Date = 10/24/15 Pct Recovery = 36% Analysis Date = 10/24/15 Pct Recovery = 36% Analysis Date = 10/19/15 Pct Recovery = 36% Analysis Date = 10/19/15 Pct Recovery = 36% Analysis Date = 10/14/15 Pct Recovery = 36% Analysis Date = 10/14/15 Pct Recovery = 36% Analysis Date = 10/09/15 Pct Recovery = 36% Analysis Date = 10/09/15 Pct Recovery = 36% Analysis Date = 10/05/15 Pct Recovery = 36% Analysis Date = 10/05/15 Pct Recovery = 36% Analysis Date = 09/30/15 Pct Recovery = 36% Analysis Date = 09/30/15 Pct Recovery = 36% Analysis Date = 09/25/15 Pct Recovery = 36% Analysis Date = 09/25/15 Pct Recovery = 36% Analysis Date = 09/20/15 Pct Recovery = 36% Analysis Date = 09/20/15 Pct Recovery = 36% Analysis Date = 09/15/15 Pct Recovery = 37% Analysis Date = 09/15/15 Pct Recovery = 37% Analysis Date = 09/10/15 Pct Recovery = 37% Analysis Date = 09/10/15 Pct Recovery = 37% Analysis Date = 09/06/15 Pct Recovery = 37% Analysis Date = 09/06/15 Pct Recovery = 37% Analysis Date = 09/01/15 Pct Recovery = 37% Analysis Date = 09/01/15 Pct Recovery = 37% Analysis Date = 08/27/15 Pct Recovery = 37% Analysis Date = 08/27/15 Pct Recovery = 37% Analysis Date = 08/22/15 Pct Recovery = 37% Analysis Date = 08/22/15 Pct Recovery = 37% Analysis Date = 08/17/15 Pct Recovery = 37% Analysis Date = 08/17/15 Pct Recovery = 37% Analysis Date = 08/13/15 Pct Recovery = 37% Analysis Date = 08/13/15 Pct Recovery = 37% Analysis Date = 08/08/15 Pct Recovery = 37% Analysis Date = 08/08/15 Pct Recovery = 37% Analysis Date = 08/03/15 Pct Recovery = 37% Analysis Date = 08/03/15 Pct Recovery = 37% Analysis Date = 07/29/15 Pct Recovery = 37% Analysis Date = 07/29/15 Pct Recovery = 37% Analysis Date = 07/24/15 Pct Recovery = 37% Analysis Date = 07/24/15 Pct Recovery = 37% Analysis Date = 07/19/15 Pct Recovery = 37% Analysis Date = 07/19/15 Pct Recovery = 37% Analysis Date = 07/15/15 Pct Recovery = 37% Analysis Date = 07/15/15 Pct Recovery = 37% Analysis Date = 07/10/15 Pct Recovery = 37% Analysis Date = 07/10/15 Pct Recovery = 37% Analysis Date = 07/05/15 Pct Recovery = 37% Analysis Date = 07/05/15 Pct Recovery = 37% Analysis Date = 06/30/15 Pct Recovery = 37% Analysis Date = 06/30/15 Pct Recovery = 37% Analysis Date = 06/25/15 Pct Recovery = 37% Analysis Date = 06/25/15 Pct Recovery = 37% Analysis Date = 06/21/15 Pct Recovery = 36% Analysis Date = 06/21/15 Pct Recovery = 36% Analysis Date = 06/16/15 Pct Recovery = 36% Analysis Date = 06/16/15 Pct Recovery = 36% Analysis Date = 06/11/15 Pct Recovery = 36% Analysis Date = 06/11/15 Pct Recovery = 36% Analysis Date = 06/06/15 Pct Recovery = 36% Analysis Date = 06/06/15 Pct Recovery = 36% Analysis Date = 06/01/15 Pct Recovery = 36% Analysis Date = 06/01/15 Pct Recovery = 36% Analysis Date = 05/27/15 Pct Recovery = 36% Analysis Date = 05/27/15 Pct Recovery = 36% Analysis Date = 05/23/15 Pct Recovery = 36% Analysis Date = 05/23/15 Pct Recovery = 36% Analysis Date = 05/18/15 Pct Recovery = 36% Analysis Date = 05/18/15 Pct Recovery = 36% Analysis Date = 05/13/15 Pct Recovery = 36% Analysis Date = 05/13/15 Pct Recovery = 36% Analysis Date = 05/08/15 Pct Recovery = 36% Analysis Date = 05/08/15 Pct Recovery = 36% Analysis Date = 05/03/15 Pct Recovery = 36% Analysis Date = 05/03/15 Pct Recovery = 36% Analysis Date = 04/29/15 Pct Recovery = 36% Analysis Date = 04/29/15 Pct Recovery = 36% Analysis Date = 04/24/15 Pct Recovery = 36% Analysis Date = 04/24/15 Pct Recovery = 36% Analysis Date = 04/19/15 Pct Recovery = 36% Analysis Date = 04/19/15 Pct Recovery = 36% Analysis Date = 04/14/15 Pct Recovery = 36% Analysis Date = 04/14/15 Pct Recovery = 36% Analysis Date = 04/09/15 Pct Recovery = 36% Analysis Date = 04/09/15 Pct Recovery = 36% Analysis Date = 04/04/15 Pct Recovery = 36% Analysis Date = 04/04/15 Pct Recovery = 36% Analysis Date = 03/31/15 Pct Recovery = 36% Analysis Date = 03/31/15 Pct Recovery = 36% Analysis Date = 03/26/15 Pct Recovery = 36% Analysis Date = 03/26/15 Pct Recovery = 36% Analysis Date = 03/21/15 Pct Recovery = 36% Analysis Date = 03/21/15 Pct Recovery = 36% Analysis Date = 03/16/15 Pct Recovery = 36% Analysis Date = 03/16/15 Pct Recovery = 36% Analysis Date = 03/11/15 Pct Recovery = 36% Analysis Date = 03/11/15 Pct Recovery = 36% Analysis Date = 03/07/15 Pct Recovery = 36% Analysis Date = 03/07/15 Pct Recovery = 36% Analysis Date = 03/02/15 Pct Recovery = 36% Analysis Date = 03/02/15 Pct Recovery = 36% Analysis Date = 02/25/15 Pct Recovery = 36% Analysis Date = 02/25/15 Pct Recovery = 36% Analysis Date = 02/20/15 Pct Recovery = 36% Analysis Date = 02/20/15 Pct Recovery = 36% Analysis Date = 02/15/15 Pct Recovery = 36% Analysis Date = 02/15/15 Pct Recovery = 36% Analysis Date = 02/10/15 Pct Recovery = 36% Analysis Date = 02/10/15 Pct Recovery = 36% Analysis Date = 02/06/15 Pct Recovery = 36% Analysis Date = 02/06/15 Pct Recovery = 36% Analysis Date = 02/01/15 Pct Recovery = 36% Analysis Date = 02/01/15 Pct Recovery = 36% Analysis Date = 01/27/15 Pct Recovery = 36% Analysis Date = 01/27/15 Pct Recovery = 36% Analysis Date = 01/22/15 Pct Recovery = 36% Analysis Date = 01/22/15 Pct Recovery = 36% Analysis Date = 01/17/15 Pct Recovery = 36% Analysis Date = 01/17/15 Pct Recovery = 36% Analysis Date = 01/12/15 Pct Recovery = 36% Analysis Date = 01/12/15 Pct Recovery = 36% Analysis Date = 01/08/15 Pct Recovery = 36% Analysis Date = 01/08/15 Pct Recovery = 36% Analysis Date = 01/03/15 Pct Recovery = 36% Analysis Date = 01/03/15 Pct Recovery = 36% Analysis Date = 12/29/14 Pct Recovery = 35% Analysis Date = 12/29/14 Pct Recovery = 35% Analysis Date = 12/24/14 Pct Recovery = 35% Analysis Date = 12/24/14 Pct Recovery = 35% Analysis Date = 12/19/14 Pct Recovery = 35% Analysis Date = 12/19/14 Pct Recovery = 35% Analysis Date = 12/15/14 Pct Recovery = 35% Analysis Date = 12/15/14 Pct Recovery = 35% Analysis Date = 12/10/14 Pct Recovery = 35% Analysis Date = 12/10/14 Pct Recovery = 35% Analysis Date = 12/05/14 Pct Recovery = 35% Analysis Date = 12/05/14 Pct Recovery = 35% Analysis Date = 11/30/14 Pct Recovery = 35% Analysis Date = 11/30/14 Pct Recovery = 35% Analysis Date = 11/25/14 Pct Recovery = 35% Analysis Date = 11/25/14 Pct Recovery = 35% Analysis Date = 11/20/14 Pct Recovery = 35% Analysis Date = 11/20/14 Pct Recovery = 35% Analysis Date = 11/16/14 Pct Recovery = 35% Analysis Date = 11/16/14 Pct Recovery = 35% Analysis Date = 11/11/14 Pct Recovery = 35% Analysis Date = 11/11/14 Pct Recovery = 35% Analysis Date = 11/06/14 Pct Recovery = 35% Analysis Date = 11/06/14 Pct Recovery = 35% Analysis Date = 11/01/14 Pct Recovery = 35% Analysis Date = 11/01/14 Pct Recovery = 35% Analysis Date = 10/27/14 Pct Recovery = 35% Analysis Date = 10/27/14 Pct Recovery = 35% Analysis Date = 10/23/14 Pct Recovery = 35% Analysis Date = 10/23/14 Pct Recovery = 35% Analysis Date = 10/18/14 Pct Recovery = 35% Analysis Date = 10/18/14 Pct Recovery = 35% Analysis Date = 10/13/14 Pct Recovery = 35% Analysis Date = 10/13/14 Pct Recovery = 35% Analysis Date = 10/08/14 Pct Recovery = 35% Analysis Date = 10/08/14 Pct Recovery = 35% Analysis Date = 10/03/14 Pct Recovery = 35% Analysis Date = 10/03/14 Pct Recovery = 35% Analysis Date = 09/28/14 Pct Recovery = 35% Analysis Date = 09/28/14 Pct Recovery = 35% Analysis Date = 09/24/14 Pct Recovery = 35% Analysis Date = 09/24/14 Pct Recovery = 35% Analysis Date = 09/19/14 Pct Recovery = 35% Analysis Date = 09/19/14 Pct Recovery = 35% Analysis Date = 09/14/14 Pct Recovery = 35% Analysis Date = 09/14/14 Pct Recovery = 35% Analysis Date = 09/09/14 Pct Recovery = 35% Analysis Date = 09/09/14 Pct Recovery = 35% Analysis Date = 09/04/14 Pct Recovery = 35% Analysis Date = 09/04/14 Pct Recovery = 35% Analysis Date = 08/31/14 Pct Recovery = 35% Analysis Date = 08/31/14 Pct Recovery = 35% Analysis Date = 08/26/14 Pct Recovery = 35% Analysis Date = 08/26/14 Pct Recovery = 35% Analysis Date = 08/21/14 Pct Recovery = 35% Analysis Date = 08/21/14 Pct Recovery = 35% Analysis Date = 08/16/14 Pct Recovery = 35% Analysis Date = 08/16/14 Pct Recovery = 35% Analysis Date = 08/11/14 Pct Recovery = 35% Analysis Date = 08/11/14 Pct Recovery = 35% Analysis Date = 08/06/14 Pct Recovery = 34% Analysis Date = 08/06/14 Pct Recovery = 34% Analysis Date = 08/02/14 Pct Recovery = 34% Analysis Date = 08/02/14 Pct Recovery = 34% Analysis Date = 07/28/14 Pct Recovery = 34% Analysis Date = 07/28/14 Pct Recovery = 34% Analysis Date = 07/23/14 Pct Recovery = 34% Analysis Date = 07/23/14 Pct Recovery = 34% Analysis Date = 07/18/14 Pct Recovery = 34% Analysis Date = 07/18/14 Pct Recovery = 34% Analysis Date = 07/13/14 Pct Recovery = 34% Analysis Date = 07/13/14 Pct Recovery = 34% Analysis Date = 07/09/14 Pct Recovery = 34% Analysis Date = 07/09/14 Pct Recovery = 34% Analysis Date = 07/04/14 Pct Recovery = 34% Analysis Date = 07/04/14 Pct Recovery = 34% Analysis Date = 06/29/14 Pct Recovery = 34% Analysis Date = 06/29/14 Pct Recovery = 34% Analysis Date = 06/24/14 Pct Recovery = 34% Analysis Date = 06/24/14 Pct Recovery = 34% Analysis Date = 06/19/14 Pct Recovery = 34% Analysis Date = 06/19/14 Pct Recovery = 34% Analysis Date = 06/14/14 Pct Recovery = 34% Analysis Date = 06/14/14 Pct Recovery = 34% Analysis Date = 06/10/14 Pct Recovery = 34% Analysis Date = 06/10/14 Pct Recovery = 34% Analysis Date = 06/05/14 Pct Recovery = 34% Analysis Date = 06/05/14 Pct Recovery = 34% Analysis Date = 05/31/14 Pct Recovery = 34% Analysis Date = 05/31/14 Pct Recovery = 34% Analysis Date = 05/26/14 Pct Recovery = 34% Analysis Date = 05/26/14 Pct Recovery = 34% Analysis Date = 05/21/14 Pct Recovery = 34% Analysis Date = 05/21/14 Pct Recovery = 34% Analysis Date = 05/17/14 Pct Recovery = 34% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
METOPROLOL

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 2 32% 4% 32% 5%
>= Reporting Level 71 36% 5% 35% 5%
Total 73 36% 5% 35% 4%

Sample Statistics
METOPROLOL

Characteristic N % % Basis
Plotted 73 97% Spiked
Estimated Values 4 5% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 1 1% Spiked
Spiked 75 .  
False Negatives 1 1% 1 out of 75
Not Spiked 40 .  
False Positives 0 0% 0 out of 40

BQS OBSP Determination:
MORPHINE
METHOD: 2440 , TESTIDCODE: 67458LCM56
Open Data Set

Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 236% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 240% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 77% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 76% Analysis Date = 11/24/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 89% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 68% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 76% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 74% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 81% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-04: 15 µl & Abs 041814: 15 µl Pct Recovery = 71% Analysis Date = 02/06/15 SpikeMix = Abs 041814: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 60% Analysis Date = 07/12/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 83% Analysis Date = 06/22/14 SpikeMix = Abs 041814: 60 µl & Abs 041614: 60 µl Pct Recovery = 108% Analysis Date = 05/21/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 69% Analysis Date = 07/30/15 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 44% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 57% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 68% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 89% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 80% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 161% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 170% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 80% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 75% Analysis Date = 04/10/15 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 57% Analysis Date = 11/04/14 SpikeMix = Abs 041814: 8 µl & ERA 0318-14-02: 8 µl Pct Recovery = 75% Analysis Date = 10/11/14 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 54% Analysis Date = 10/10/14 SpikeMix = Abs 041714: 30 µl & Abs 041814: 30 µl Pct Recovery = 68% Analysis Date = 10/10/14 SpikeMix = Abs 041814: 30 µl & ERA 0318-14-02: 30 µl Pct Recovery = 75% Analysis Date = 07/13/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 77% Analysis Date = 05/30/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 92% Analysis Date = 06/26/15 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 58% Analysis Date = 11/18/16 SpikeMix = ERA 04281604: 80 µl & ERA 04281603: 80 µl Pct Recovery = 79% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & ERA 04281604: 80 µl Pct Recovery = 70% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 70% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 85% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 62% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 88% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 75% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 84% Analysis Date = 01/18/17 Pct Recovery = 142% Analysis Date = 01/14/17 Pct Recovery = 139% Analysis Date = 01/14/17 Pct Recovery = 139% Analysis Date = 01/09/17 Pct Recovery = 136% Analysis Date = 01/09/17 Pct Recovery = 136% Analysis Date = 01/04/17 Pct Recovery = 132% Analysis Date = 01/04/17 Pct Recovery = 132% Analysis Date = 12/30/16 Pct Recovery = 129% Analysis Date = 12/30/16 Pct Recovery = 129% Analysis Date = 12/25/16 Pct Recovery = 126% Analysis Date = 12/25/16 Pct Recovery = 126% Analysis Date = 12/20/16 Pct Recovery = 123% Analysis Date = 12/20/16 Pct Recovery = 123% Analysis Date = 12/15/16 Pct Recovery = 120% Analysis Date = 12/15/16 Pct Recovery = 120% Analysis Date = 12/11/16 Pct Recovery = 117% Analysis Date = 12/11/16 Pct Recovery = 117% Analysis Date = 12/06/16 Pct Recovery = 114% Analysis Date = 12/06/16 Pct Recovery = 114% Analysis Date = 12/01/16 Pct Recovery = 111% Analysis Date = 12/01/16 Pct Recovery = 111% Analysis Date = 11/26/16 Pct Recovery = 108% Analysis Date = 11/26/16 Pct Recovery = 108% Analysis Date = 11/21/16 Pct Recovery = 105% Analysis Date = 11/21/16 Pct Recovery = 105% Analysis Date = 11/16/16 Pct Recovery = 102% Analysis Date = 11/16/16 Pct Recovery = 102% Analysis Date = 11/11/16 Pct Recovery = 98% Analysis Date = 11/11/16 Pct Recovery = 98% Analysis Date = 11/06/16 Pct Recovery = 94% Analysis Date = 11/06/16 Pct Recovery = 94% Analysis Date = 11/02/16 Pct Recovery = 91% Analysis Date = 11/02/16 Pct Recovery = 91% Analysis Date = 10/28/16 Pct Recovery = 87% Analysis Date = 10/28/16 Pct Recovery = 87% Analysis Date = 10/23/16 Pct Recovery = 87% Analysis Date = 10/23/16 Pct Recovery = 87% Analysis Date = 10/18/16 Pct Recovery = 87% Analysis Date = 10/18/16 Pct Recovery = 87% Analysis Date = 10/13/16 Pct Recovery = 87% Analysis Date = 10/13/16 Pct Recovery = 87% Analysis Date = 10/08/16 Pct Recovery = 87% Analysis Date = 10/08/16 Pct Recovery = 87% Analysis Date = 10/03/16 Pct Recovery = 87% Analysis Date = 10/03/16 Pct Recovery = 87% Analysis Date = 09/28/16 Pct Recovery = 87% Analysis Date = 09/28/16 Pct Recovery = 87% Analysis Date = 09/24/16 Pct Recovery = 87% Analysis Date = 09/24/16 Pct Recovery = 87% Analysis Date = 09/19/16 Pct Recovery = 87% Analysis Date = 09/19/16 Pct Recovery = 87% Analysis Date = 09/14/16 Pct Recovery = 88% Analysis Date = 09/14/16 Pct Recovery = 88% Analysis Date = 09/09/16 Pct Recovery = 88% Analysis Date = 09/09/16 Pct Recovery = 88% Analysis Date = 09/04/16 Pct Recovery = 89% Analysis Date = 09/04/16 Pct Recovery = 89% Analysis Date = 08/30/16 Pct Recovery = 90% Analysis Date = 08/30/16 Pct Recovery = 90% Analysis Date = 08/25/16 Pct Recovery = 91% Analysis Date = 08/25/16 Pct Recovery = 91% Analysis Date = 08/21/16 Pct Recovery = 92% Analysis Date = 08/21/16 Pct Recovery = 92% Analysis Date = 08/16/16 Pct Recovery = 93% Analysis Date = 08/16/16 Pct Recovery = 93% Analysis Date = 08/11/16 Pct Recovery = 94% Analysis Date = 08/11/16 Pct Recovery = 94% Analysis Date = 08/06/16 Pct Recovery = 94% Analysis Date = 08/06/16 Pct Recovery = 94% Analysis Date = 08/01/16 Pct Recovery = 93% Analysis Date = 08/01/16 Pct Recovery = 93% Analysis Date = 07/27/16 Pct Recovery = 93% Analysis Date = 07/27/16 Pct Recovery = 93% Analysis Date = 07/22/16 Pct Recovery = 93% Analysis Date = 07/22/16 Pct Recovery = 93% Analysis Date = 07/17/16 Pct Recovery = 92% Analysis Date = 07/17/16 Pct Recovery = 92% Analysis Date = 07/13/16 Pct Recovery = 92% Analysis Date = 07/13/16 Pct Recovery = 92% Analysis Date = 07/08/16 Pct Recovery = 91% Analysis Date = 07/08/16 Pct Recovery = 91% Analysis Date = 07/03/16 Pct Recovery = 91% Analysis Date = 07/03/16 Pct Recovery = 91% Analysis Date = 06/28/16 Pct Recovery = 91% Analysis Date = 06/28/16 Pct Recovery = 91% Analysis Date = 06/23/16 Pct Recovery = 90% Analysis Date = 06/23/16 Pct Recovery = 90% Analysis Date = 06/18/16 Pct Recovery = 90% Analysis Date = 06/18/16 Pct Recovery = 90% Analysis Date = 06/13/16 Pct Recovery = 90% Analysis Date = 06/13/16 Pct Recovery = 90% Analysis Date = 06/08/16 Pct Recovery = 89% Analysis Date = 06/08/16 Pct Recovery = 89% Analysis Date = 06/04/16 Pct Recovery = 89% Analysis Date = 06/04/16 Pct Recovery = 89% Analysis Date = 05/30/16 Pct Recovery = 88% Analysis Date = 05/30/16 Pct Recovery = 88% Analysis Date = 05/25/16 Pct Recovery = 88% Analysis Date = 05/25/16 Pct Recovery = 88% Analysis Date = 05/20/16 Pct Recovery = 88% Analysis Date = 05/20/16 Pct Recovery = 88% Analysis Date = 05/15/16 Pct Recovery = 87% Analysis Date = 05/15/16 Pct Recovery = 87% Analysis Date = 05/10/16 Pct Recovery = 87% Analysis Date = 05/10/16 Pct Recovery = 87% Analysis Date = 05/05/16 Pct Recovery = 86% Analysis Date = 05/05/16 Pct Recovery = 86% Analysis Date = 05/01/16 Pct Recovery = 86% Analysis Date = 05/01/16 Pct Recovery = 86% Analysis Date = 04/26/16 Pct Recovery = 86% Analysis Date = 04/26/16 Pct Recovery = 86% Analysis Date = 04/21/16 Pct Recovery = 85% Analysis Date = 04/21/16 Pct Recovery = 85% Analysis Date = 04/16/16 Pct Recovery = 85% Analysis Date = 04/16/16 Pct Recovery = 85% Analysis Date = 04/11/16 Pct Recovery = 84% Analysis Date = 04/11/16 Pct Recovery = 84% Analysis Date = 04/06/16 Pct Recovery = 84% Analysis Date = 04/06/16 Pct Recovery = 84% Analysis Date = 04/01/16 Pct Recovery = 84% Analysis Date = 04/01/16 Pct Recovery = 84% Analysis Date = 03/27/16 Pct Recovery = 83% Analysis Date = 03/27/16 Pct Recovery = 83% Analysis Date = 03/23/16 Pct Recovery = 83% Analysis Date = 03/23/16 Pct Recovery = 83% Analysis Date = 03/18/16 Pct Recovery = 82% Analysis Date = 03/18/16 Pct Recovery = 82% Analysis Date = 03/13/16 Pct Recovery = 82% Analysis Date = 03/13/16 Pct Recovery = 82% Analysis Date = 03/08/16 Pct Recovery = 82% Analysis Date = 03/08/16 Pct Recovery = 82% Analysis Date = 03/03/16 Pct Recovery = 81% Analysis Date = 03/03/16 Pct Recovery = 81% Analysis Date = 02/27/16 Pct Recovery = 81% Analysis Date = 02/27/16 Pct Recovery = 81% Analysis Date = 02/22/16 Pct Recovery = 80% Analysis Date = 02/22/16 Pct Recovery = 80% Analysis Date = 02/17/16 Pct Recovery = 80% Analysis Date = 02/17/16 Pct Recovery = 80% Analysis Date = 02/13/16 Pct Recovery = 80% Analysis Date = 02/13/16 Pct Recovery = 80% Analysis Date = 02/08/16 Pct Recovery = 79% Analysis Date = 02/08/16 Pct Recovery = 79% Analysis Date = 02/03/16 Pct Recovery = 79% Analysis Date = 02/03/16 Pct Recovery = 79% Analysis Date = 01/29/16 Pct Recovery = 78% Analysis Date = 01/29/16 Pct Recovery = 78% Analysis Date = 01/24/16 Pct Recovery = 78% Analysis Date = 01/24/16 Pct Recovery = 78% Analysis Date = 01/19/16 Pct Recovery = 78% Analysis Date = 01/19/16 Pct Recovery = 78% Analysis Date = 01/14/16 Pct Recovery = 77% Analysis Date = 01/14/16 Pct Recovery = 77% Analysis Date = 01/10/16 Pct Recovery = 77% Analysis Date = 01/10/16 Pct Recovery = 77% Analysis Date = 01/05/16 Pct Recovery = 77% Analysis Date = 01/05/16 Pct Recovery = 77% Analysis Date = 12/31/15 Pct Recovery = 76% Analysis Date = 12/31/15 Pct Recovery = 76% Analysis Date = 12/26/15 Pct Recovery = 76% Analysis Date = 12/26/15 Pct Recovery = 76% Analysis Date = 12/21/15 Pct Recovery = 75% Analysis Date = 12/21/15 Pct Recovery = 75% Analysis Date = 12/16/15 Pct Recovery = 75% Analysis Date = 12/16/15 Pct Recovery = 75% Analysis Date = 12/11/15 Pct Recovery = 75% Analysis Date = 12/11/15 Pct Recovery = 75% Analysis Date = 12/06/15 Pct Recovery = 74% Analysis Date = 12/06/15 Pct Recovery = 74% Analysis Date = 12/02/15 Pct Recovery = 74% Analysis Date = 12/02/15 Pct Recovery = 74% Analysis Date = 11/27/15 Pct Recovery = 73% Analysis Date = 11/27/15 Pct Recovery = 73% Analysis Date = 11/22/15 Pct Recovery = 73% Analysis Date = 11/22/15 Pct Recovery = 73% Analysis Date = 11/17/15 Pct Recovery = 73% Analysis Date = 11/17/15 Pct Recovery = 73% Analysis Date = 11/12/15 Pct Recovery = 72% Analysis Date = 11/12/15 Pct Recovery = 72% Analysis Date = 11/07/15 Pct Recovery = 72% Analysis Date = 11/07/15 Pct Recovery = 72% Analysis Date = 11/02/15 Pct Recovery = 72% Analysis Date = 11/02/15 Pct Recovery = 72% Analysis Date = 10/28/15 Pct Recovery = 72% Analysis Date = 10/28/15 Pct Recovery = 72% Analysis Date = 10/24/15 Pct Recovery = 71% Analysis Date = 10/24/15 Pct Recovery = 71% Analysis Date = 10/19/15 Pct Recovery = 71% Analysis Date = 10/19/15 Pct Recovery = 71% Analysis Date = 10/14/15 Pct Recovery = 71% Analysis Date = 10/14/15 Pct Recovery = 71% Analysis Date = 10/09/15 Pct Recovery = 71% Analysis Date = 10/09/15 Pct Recovery = 71% Analysis Date = 10/04/15 Pct Recovery = 70% Analysis Date = 10/04/15 Pct Recovery = 70% Analysis Date = 09/29/15 Pct Recovery = 70% Analysis Date = 09/29/15 Pct Recovery = 70% Analysis Date = 09/24/15 Pct Recovery = 70% Analysis Date = 09/24/15 Pct Recovery = 70% Analysis Date = 09/19/15 Pct Recovery = 70% Analysis Date = 09/19/15 Pct Recovery = 70% Analysis Date = 09/15/15 Pct Recovery = 69% Analysis Date = 09/15/15 Pct Recovery = 69% Analysis Date = 09/10/15 Pct Recovery = 69% Analysis Date = 09/10/15 Pct Recovery = 69% Analysis Date = 09/05/15 Pct Recovery = 69% Analysis Date = 09/05/15 Pct Recovery = 69% Analysis Date = 08/31/15 Pct Recovery = 69% Analysis Date = 08/31/15 Pct Recovery = 69% Analysis Date = 08/26/15 Pct Recovery = 68% Analysis Date = 08/26/15 Pct Recovery = 68% Analysis Date = 08/21/15 Pct Recovery = 68% Analysis Date = 08/21/15 Pct Recovery = 68% Analysis Date = 08/16/15 Pct Recovery = 68% Analysis Date = 08/16/15 Pct Recovery = 68% Analysis Date = 08/12/15 Pct Recovery = 67% Analysis Date = 08/12/15 Pct Recovery = 67% Analysis Date = 08/07/15 Pct Recovery = 67% Analysis Date = 08/07/15 Pct Recovery = 67% Analysis Date = 08/02/15 Pct Recovery = 67% Analysis Date = 08/02/15 Pct Recovery = 67% Analysis Date = 07/28/15 Pct Recovery = 67% Analysis Date = 07/28/15 Pct Recovery = 67% Analysis Date = 07/23/15 Pct Recovery = 66% Analysis Date = 07/23/15 Pct Recovery = 66% Analysis Date = 07/18/15 Pct Recovery = 66% Analysis Date = 07/18/15 Pct Recovery = 66% Analysis Date = 07/13/15 Pct Recovery = 66% Analysis Date = 07/13/15 Pct Recovery = 66% Analysis Date = 07/08/15 Pct Recovery = 66% Analysis Date = 07/08/15 Pct Recovery = 66% Analysis Date = 07/04/15 Pct Recovery = 65% Analysis Date = 07/04/15 Pct Recovery = 65% Analysis Date = 06/29/15 Pct Recovery = 65% Analysis Date = 06/29/15 Pct Recovery = 65% Analysis Date = 06/24/15 Pct Recovery = 65% Analysis Date = 06/24/15 Pct Recovery = 65% Analysis Date = 06/19/15 Pct Recovery = 65% Analysis Date = 06/19/15 Pct Recovery = 65% Analysis Date = 06/14/15 Pct Recovery = 65% Analysis Date = 06/14/15 Pct Recovery = 65% Analysis Date = 06/09/15 Pct Recovery = 65% Analysis Date = 06/09/15 Pct Recovery = 65% Analysis Date = 06/04/15 Pct Recovery = 65% Analysis Date = 06/04/15 Pct Recovery = 65% Analysis Date = 05/30/15 Pct Recovery = 66% Analysis Date = 05/30/15 Pct Recovery = 66% Analysis Date = 05/26/15 Pct Recovery = 66% Analysis Date = 05/26/15 Pct Recovery = 66% Analysis Date = 05/21/15 Pct Recovery = 66% Analysis Date = 05/21/15 Pct Recovery = 66% Analysis Date = 05/16/15 Pct Recovery = 66% Analysis Date = 05/16/15 Pct Recovery = 66% Analysis Date = 05/11/15 Pct Recovery = 66% Analysis Date = 05/11/15 Pct Recovery = 66% Analysis Date = 05/06/15 Pct Recovery = 66% Analysis Date = 05/06/15 Pct Recovery = 66% Analysis Date = 05/01/15 Pct Recovery = 66% Analysis Date = 05/01/15 Pct Recovery = 66% Analysis Date = 04/26/15 Pct Recovery = 66% Analysis Date = 04/26/15 Pct Recovery = 66% Analysis Date = 04/22/15 Pct Recovery = 66% Analysis Date = 04/22/15 Pct Recovery = 66% Analysis Date = 04/17/15 Pct Recovery = 67% Analysis Date = 04/17/15 Pct Recovery = 67% Analysis Date = 04/12/15 Pct Recovery = 67% Analysis Date = 04/12/15 Pct Recovery = 67% Analysis Date = 04/07/15 Pct Recovery = 67% Analysis Date = 04/07/15 Pct Recovery = 67% Analysis Date = 04/02/15 Pct Recovery = 67% Analysis Date = 04/02/15 Pct Recovery = 67% Analysis Date = 03/28/15 Pct Recovery = 67% Analysis Date = 03/28/15 Pct Recovery = 67% Analysis Date = 03/23/15 Pct Recovery = 67% Analysis Date = 03/23/15 Pct Recovery = 67% Analysis Date = 03/18/15 Pct Recovery = 67% Analysis Date = 03/18/15 Pct Recovery = 67% Analysis Date = 03/14/15 Pct Recovery = 67% Analysis Date = 03/14/15 Pct Recovery = 67% Analysis Date = 03/09/15 Pct Recovery = 67% Analysis Date = 03/09/15 Pct Recovery = 67% Analysis Date = 03/04/15 Pct Recovery = 68% Analysis Date = 03/04/15 Pct Recovery = 68% Analysis Date = 02/27/15 Pct Recovery = 68% Analysis Date = 02/27/15 Pct Recovery = 68% Analysis Date = 02/22/15 Pct Recovery = 68% Analysis Date = 02/22/15 Pct Recovery = 68% Analysis Date = 02/17/15 Pct Recovery = 68% Analysis Date = 02/17/15 Pct Recovery = 68% Analysis Date = 02/12/15 Pct Recovery = 68% Analysis Date = 02/12/15 Pct Recovery = 68% Analysis Date = 02/07/15 Pct Recovery = 68% Analysis Date = 02/07/15 Pct Recovery = 68% Analysis Date = 02/03/15 Pct Recovery = 68% Analysis Date = 02/03/15 Pct Recovery = 68% Analysis Date = 01/29/15 Pct Recovery = 69% Analysis Date = 01/29/15 Pct Recovery = 69% Analysis Date = 01/24/15 Pct Recovery = 69% Analysis Date = 01/24/15 Pct Recovery = 69% Analysis Date = 01/19/15 Pct Recovery = 69% Analysis Date = 01/19/15 Pct Recovery = 69% Analysis Date = 01/14/15 Pct Recovery = 69% Analysis Date = 01/14/15 Pct Recovery = 69% Analysis Date = 01/09/15 Pct Recovery = 70% Analysis Date = 01/09/15 Pct Recovery = 70% Analysis Date = 01/04/15 Pct Recovery = 70% Analysis Date = 01/04/15 Pct Recovery = 70% Analysis Date = 12/31/14 Pct Recovery = 70% Analysis Date = 12/31/14 Pct Recovery = 70% Analysis Date = 12/26/14 Pct Recovery = 70% Analysis Date = 12/26/14 Pct Recovery = 70% Analysis Date = 12/21/14 Pct Recovery = 71% Analysis Date = 12/21/14 Pct Recovery = 71% Analysis Date = 12/16/14 Pct Recovery = 71% Analysis Date = 12/16/14 Pct Recovery = 71% Analysis Date = 12/11/14 Pct Recovery = 71% Analysis Date = 12/11/14 Pct Recovery = 71% Analysis Date = 12/06/14 Pct Recovery = 71% Analysis Date = 12/06/14 Pct Recovery = 71% Analysis Date = 12/01/14 Pct Recovery = 72% Analysis Date = 12/01/14 Pct Recovery = 72% Analysis Date = 11/26/14 Pct Recovery = 72% Analysis Date = 11/26/14 Pct Recovery = 72% Analysis Date = 11/22/14 Pct Recovery = 72% Analysis Date = 11/22/14 Pct Recovery = 72% Analysis Date = 11/17/14 Pct Recovery = 72% Analysis Date = 11/17/14 Pct Recovery = 72% Analysis Date = 11/12/14 Pct Recovery = 72% Analysis Date = 11/12/14 Pct Recovery = 72% Analysis Date = 11/07/14 Pct Recovery = 73% Analysis Date = 11/07/14 Pct Recovery = 73% Analysis Date = 11/02/14 Pct Recovery = 73% Analysis Date = 11/02/14 Pct Recovery = 73% Analysis Date = 10/28/14 Pct Recovery = 73% Analysis Date = 10/28/14 Pct Recovery = 73% Analysis Date = 10/23/14 Pct Recovery = 73% Analysis Date = 10/23/14 Pct Recovery = 73% Analysis Date = 10/18/14 Pct Recovery = 74% Analysis Date = 10/18/14 Pct Recovery = 74% Analysis Date = 10/14/14 Pct Recovery = 74% Analysis Date = 10/14/14 Pct Recovery = 74% Analysis Date = 10/09/14 Pct Recovery = 74% Analysis Date = 10/09/14 Pct Recovery = 74% Analysis Date = 10/04/14 Pct Recovery = 74% Analysis Date = 10/04/14 Pct Recovery = 74% Analysis Date = 09/29/14 Pct Recovery = 75% Analysis Date = 09/29/14 Pct Recovery = 75% Analysis Date = 09/24/14 Pct Recovery = 75% Analysis Date = 09/24/14 Pct Recovery = 75% Analysis Date = 09/19/14 Pct Recovery = 75% Analysis Date = 09/19/14 Pct Recovery = 75% Analysis Date = 09/14/14 Pct Recovery = 76% Analysis Date = 09/14/14 Pct Recovery = 76% Analysis Date = 09/10/14 Pct Recovery = 76% Analysis Date = 09/10/14 Pct Recovery = 76% Analysis Date = 09/05/14 Pct Recovery = 76% Analysis Date = 09/05/14 Pct Recovery = 76% Analysis Date = 08/31/14 Pct Recovery = 76% Analysis Date = 08/31/14 Pct Recovery = 76% Analysis Date = 08/26/14 Pct Recovery = 77% Analysis Date = 08/26/14 Pct Recovery = 77% Analysis Date = 08/21/14 Pct Recovery = 77% Analysis Date = 08/21/14 Pct Recovery = 77% Analysis Date = 08/16/14 Pct Recovery = 77% Analysis Date = 08/16/14 Pct Recovery = 77% Analysis Date = 08/11/14 Pct Recovery = 78% Analysis Date = 08/11/14 Pct Recovery = 78% Analysis Date = 08/06/14 Pct Recovery = 78% Analysis Date = 08/06/14 Pct Recovery = 78% Analysis Date = 08/02/14 Pct Recovery = 78% Analysis Date = 08/02/14 Pct Recovery = 78% Analysis Date = 07/28/14 Pct Recovery = 78% Analysis Date = 07/28/14 Pct Recovery = 78% Analysis Date = 07/23/14 Pct Recovery = 79% Analysis Date = 07/23/14 Pct Recovery = 79% Analysis Date = 07/18/14 Pct Recovery = 79% Analysis Date = 07/18/14 Pct Recovery = 79% Analysis Date = 07/13/14 Pct Recovery = 79% Analysis Date = 07/13/14 Pct Recovery = 79% Analysis Date = 07/08/14 Pct Recovery = 80% Analysis Date = 07/08/14 Pct Recovery = 80% Analysis Date = 07/03/14 Pct Recovery = 80% Analysis Date = 07/03/14 Pct Recovery = 80% Analysis Date = 06/28/14 Pct Recovery = 80% Analysis Date = 06/28/14 Pct Recovery = 80% Analysis Date = 06/24/14 Pct Recovery = 80% Analysis Date = 06/24/14 Pct Recovery = 80% Analysis Date = 06/19/14 Pct Recovery = 81% Analysis Date = 06/19/14 Pct Recovery = 81% Analysis Date = 06/14/14 Pct Recovery = 81% Analysis Date = 06/14/14 Pct Recovery = 81% Analysis Date = 06/09/14 Pct Recovery = 81% Analysis Date = 06/09/14 Pct Recovery = 81% Analysis Date = 06/04/14 Pct Recovery = 82% Analysis Date = 06/04/14 Pct Recovery = 82% Analysis Date = 05/30/14 Pct Recovery = 82% Analysis Date = 05/30/14 Pct Recovery = 82% Analysis Date = 05/25/14 Pct Recovery = 82% Analysis Date = 05/25/14 Pct Recovery = 82% Analysis Date = 05/21/14 Pct Recovery = 83% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
MORPHINE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 10 109% 68% 82% 13%
>= Reporting Level 29 80% 27% 75% 10%
Total 39 87% 43% 76% 13%

Sample Statistics
MORPHINE

Characteristic N % % Basis
Plotted 39 76% Spiked
Estimated Values 3 6% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 2 4% Spiked
Spiked 51 .  
False Negatives 10 20% 10 out of 51
Not Spiked 64 .  
False Positives 0 0% 0 out of 64

BQS OBSP Determination:
NADALOL
METHOD: 2440 , TESTIDCODE: 68006LCM56
Open Data Set

Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 77% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 79% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 80 µl & ERA 0406-15-08: 80 µl Pct Recovery = 86% Analysis Date = 11/05/15 SpikeMix = ERA 0406-15-08: 80 µl & Abs 052215: 80 µl Pct Recovery = 63% Analysis Date = 11/24/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 100% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 80 µl & Abs 051315: 80 µl Pct Recovery = 67% Analysis Date = 10/01/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 148% Analysis Date = 11/18/16 SpikeMix = ERA 04281604: 80 µl & ERA 04281603: 80 µl Pct Recovery = 74% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & ERA 04281604: 80 µl Pct Recovery = 71% Analysis Date = 09/24/16 SpikeMix = Crescent EN160610015: 80 µl & Abs 061416: 80 µl Pct Recovery = 109% Analysis Date = 09/24/16 SpikeMix = Abs 061416: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 111% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 81% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 81% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 77% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 78% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-04: 15 µl & Abs 041814: 15 µl Pct Recovery = 79% Analysis Date = 12/06/14 SpikeMix = ERA 0318-14-02: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 72% Analysis Date = 10/25/14 SpikeMix = Abs 041614: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 85% Analysis Date = 10/11/14 SpikeMix = ERA 0318-14-02: 60 µl & ERA 0319-14-04: 60 µl Pct Recovery = 67% Analysis Date = 08/28/14 SpikeMix = ERA 0319-14-04: 60 µl & ERA 0319-14-05: 60 µl Pct Recovery = 82% Analysis Date = 05/07/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 99% Analysis Date = 03/11/15 SpikeMix = ERA 0318-14-02: 15 µl & Abs 041714: 15 µl Pct Recovery = 82% Analysis Date = 01/16/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 88% Analysis Date = 12/06/14 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 67% Analysis Date = 08/21/14 SpikeMix = ERA 0318-14-02: 60 µl & Abs 041714: 60 µl Pct Recovery = 63% Analysis Date = 07/12/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 67% Analysis Date = 06/11/14 SpikeMix = Abs 041614: 60 µl & Abs 041714: 60 µl Pct Recovery = 68% Analysis Date = 05/21/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 72% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-08: 40 µl & Abs 052215: 40 µl Pct Recovery = 78% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 79% Analysis Date = 11/04/15 SpikeMix = ERA 0406-15-07A: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 53% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-08: 40 µl & ERA 0406-15-09: 40 µl Pct Recovery = 70% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 112% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 98% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-07A: 40 µl & Abs 051315: 40 µl Pct Recovery = 84% Analysis Date = 07/31/15 SpikeMix = Abs 051315: 40 µl & Abs 052215: 40 µl Pct Recovery = 75% Analysis Date = 07/30/15 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 90% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 112% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 116% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 91% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 90% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 80% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 74% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 85% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 83% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 85% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 89% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 63% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 74% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 67% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 68% Analysis Date = 04/30/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 72% Analysis Date = 04/10/15 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 73% Analysis Date = 02/10/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 86% Analysis Date = 12/07/14 SpikeMix = ERA 0318-14-02: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 73% Analysis Date = 10/11/14 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 66% Analysis Date = 11/04/14 SpikeMix = Abs 041714: 8 µl & ERA 0319-14-05: 8 µl Pct Recovery = 75% Analysis Date = 09/12/14 SpikeMix = Abs 041614: 30 µl & ERA 0319-14-04: 30 µl Pct Recovery = 71% Analysis Date = 08/16/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 58% Analysis Date = 07/13/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 65% Analysis Date = 10/10/14 SpikeMix = Abs 041714: 30 µl & Abs 041814: 30 µl Pct Recovery = 65% Analysis Date = 07/20/14 SpikeMix = ERA 0318-14-02: 30 µl & Abs 041714: 30 µl Pct Recovery = 61% Analysis Date = 06/28/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 67% Analysis Date = 05/17/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 70% Analysis Date = 04/27/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 133% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 84% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-08: 20 µl & ERA 0406-15-09: 20 µl Pct Recovery = 82% Analysis Date = 11/25/15 SpikeMix = Abs 050115: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 104% Analysis Date = 09/15/15 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 78% Analysis Date = 09/09/15 SpikeMix = ERA 0406-15-08: 20 µl & Abs 052215: 20 µl Pct Recovery = 91% Analysis Date = 02/23/16 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 72% Analysis Date = 08/11/15 SpikeMix = Abs 050115: 20 µl & Abs 051315: 20 µl Pct Recovery = 62% Analysis Date = 06/26/15 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 77% Analysis Date = 06/09/15 SpikeMix = Abs 051315: 20 µl & Abs 050115: 20 µl Pct Recovery = 68% Analysis Date = 04/09/16 SpikeMix = Abs 051315: 10 µl & ERA 0406-15-09: 10 µl Pct Recovery = 63% Analysis Date = 04/09/16 SpikeMix = Abs 051315: 10 µl & ERA 0406-15-09: 10 µl Pct Recovery = 89% Analysis Date = 01/04/17 Pct Recovery = 88% Analysis Date = 12/31/16 Pct Recovery = 88% Analysis Date = 12/31/16 Pct Recovery = 88% Analysis Date = 12/26/16 Pct Recovery = 88% Analysis Date = 12/26/16 Pct Recovery = 88% Analysis Date = 12/21/16 Pct Recovery = 88% Analysis Date = 12/21/16 Pct Recovery = 88% Analysis Date = 12/16/16 Pct Recovery = 88% Analysis Date = 12/16/16 Pct Recovery = 88% Analysis Date = 12/11/16 Pct Recovery = 88% Analysis Date = 12/11/16 Pct Recovery = 88% Analysis Date = 12/07/16 Pct Recovery = 87% Analysis Date = 12/07/16 Pct Recovery = 87% Analysis Date = 12/02/16 Pct Recovery = 87% Analysis Date = 12/02/16 Pct Recovery = 87% Analysis Date = 11/27/16 Pct Recovery = 87% Analysis Date = 11/27/16 Pct Recovery = 87% Analysis Date = 11/22/16 Pct Recovery = 87% Analysis Date = 11/22/16 Pct Recovery = 87% Analysis Date = 11/17/16 Pct Recovery = 87% Analysis Date = 11/17/16 Pct Recovery = 87% Analysis Date = 11/12/16 Pct Recovery = 87% Analysis Date = 11/12/16 Pct Recovery = 87% Analysis Date = 11/08/16 Pct Recovery = 87% Analysis Date = 11/08/16 Pct Recovery = 87% Analysis Date = 11/03/16 Pct Recovery = 87% Analysis Date = 11/03/16 Pct Recovery = 87% Analysis Date = 10/29/16 Pct Recovery = 87% Analysis Date = 10/29/16 Pct Recovery = 87% Analysis Date = 10/24/16 Pct Recovery = 87% Analysis Date = 10/24/16 Pct Recovery = 87% Analysis Date = 10/19/16 Pct Recovery = 87% Analysis Date = 10/19/16 Pct Recovery = 87% Analysis Date = 10/15/16 Pct Recovery = 86% Analysis Date = 10/15/16 Pct Recovery = 86% Analysis Date = 10/10/16 Pct Recovery = 86% Analysis Date = 10/10/16 Pct Recovery = 86% Analysis Date = 10/05/16 Pct Recovery = 86% Analysis Date = 10/05/16 Pct Recovery = 86% Analysis Date = 09/30/16 Pct Recovery = 86% Analysis Date = 09/30/16 Pct Recovery = 86% Analysis Date = 09/25/16 Pct Recovery = 86% Analysis Date = 09/25/16 Pct Recovery = 86% Analysis Date = 09/20/16 Pct Recovery = 86% Analysis Date = 09/20/16 Pct Recovery = 86% Analysis Date = 09/16/16 Pct Recovery = 86% Analysis Date = 09/16/16 Pct Recovery = 86% Analysis Date = 09/11/16 Pct Recovery = 86% Analysis Date = 09/11/16 Pct Recovery = 86% Analysis Date = 09/06/16 Pct Recovery = 86% Analysis Date = 09/06/16 Pct Recovery = 86% Analysis Date = 09/01/16 Pct Recovery = 86% Analysis Date = 09/01/16 Pct Recovery = 86% Analysis Date = 08/27/16 Pct Recovery = 86% Analysis Date = 08/27/16 Pct Recovery = 86% Analysis Date = 08/23/16 Pct Recovery = 86% Analysis Date = 08/23/16 Pct Recovery = 86% Analysis Date = 08/18/16 Pct Recovery = 86% Analysis Date = 08/18/16 Pct Recovery = 86% Analysis Date = 08/13/16 Pct Recovery = 86% Analysis Date = 08/13/16 Pct Recovery = 86% Analysis Date = 08/08/16 Pct Recovery = 85% Analysis Date = 08/08/16 Pct Recovery = 85% Analysis Date = 08/03/16 Pct Recovery = 85% Analysis Date = 08/03/16 Pct Recovery = 85% Analysis Date = 07/29/16 Pct Recovery = 85% Analysis Date = 07/29/16 Pct Recovery = 85% Analysis Date = 07/25/16 Pct Recovery = 85% Analysis Date = 07/25/16 Pct Recovery = 85% Analysis Date = 07/20/16 Pct Recovery = 85% Analysis Date = 07/20/16 Pct Recovery = 85% Analysis Date = 07/15/16 Pct Recovery = 85% Analysis Date = 07/15/16 Pct Recovery = 85% Analysis Date = 07/10/16 Pct Recovery = 85% Analysis Date = 07/10/16 Pct Recovery = 85% Analysis Date = 07/05/16 Pct Recovery = 85% Analysis Date = 07/05/16 Pct Recovery = 85% Analysis Date = 07/01/16 Pct Recovery = 85% Analysis Date = 07/01/16 Pct Recovery = 85% Analysis Date = 06/26/16 Pct Recovery = 85% Analysis Date = 06/26/16 Pct Recovery = 85% Analysis Date = 06/21/16 Pct Recovery = 85% Analysis Date = 06/21/16 Pct Recovery = 85% Analysis Date = 06/16/16 Pct Recovery = 85% Analysis Date = 06/16/16 Pct Recovery = 85% Analysis Date = 06/11/16 Pct Recovery = 85% Analysis Date = 06/11/16 Pct Recovery = 85% Analysis Date = 06/06/16 Pct Recovery = 85% Analysis Date = 06/06/16 Pct Recovery = 85% Analysis Date = 06/02/16 Pct Recovery = 85% Analysis Date = 06/02/16 Pct Recovery = 85% Analysis Date = 05/28/16 Pct Recovery = 85% Analysis Date = 05/28/16 Pct Recovery = 85% Analysis Date = 05/23/16 Pct Recovery = 85% Analysis Date = 05/23/16 Pct Recovery = 85% Analysis Date = 05/18/16 Pct Recovery = 85% Analysis Date = 05/18/16 Pct Recovery = 85% Analysis Date = 05/13/16 Pct Recovery = 85% Analysis Date = 05/13/16 Pct Recovery = 85% Analysis Date = 05/08/16 Pct Recovery = 85% Analysis Date = 05/08/16 Pct Recovery = 85% Analysis Date = 05/04/16 Pct Recovery = 85% Analysis Date = 05/04/16 Pct Recovery = 85% Analysis Date = 04/29/16 Pct Recovery = 85% Analysis Date = 04/29/16 Pct Recovery = 85% Analysis Date = 04/24/16 Pct Recovery = 85% Analysis Date = 04/24/16 Pct Recovery = 85% Analysis Date = 04/19/16 Pct Recovery = 85% Analysis Date = 04/19/16 Pct Recovery = 85% Analysis Date = 04/14/16 Pct Recovery = 85% Analysis Date = 04/14/16 Pct Recovery = 85% Analysis Date = 04/10/16 Pct Recovery = 85% Analysis Date = 04/10/16 Pct Recovery = 85% Analysis Date = 04/05/16 Pct Recovery = 85% Analysis Date = 04/05/16 Pct Recovery = 85% Analysis Date = 03/31/16 Pct Recovery = 85% Analysis Date = 03/31/16 Pct Recovery = 85% Analysis Date = 03/26/16 Pct Recovery = 85% Analysis Date = 03/26/16 Pct Recovery = 85% Analysis Date = 03/21/16 Pct Recovery = 85% Analysis Date = 03/21/16 Pct Recovery = 85% Analysis Date = 03/16/16 Pct Recovery = 85% Analysis Date = 03/16/16 Pct Recovery = 85% Analysis Date = 03/12/16 Pct Recovery = 85% Analysis Date = 03/12/16 Pct Recovery = 85% Analysis Date = 03/07/16 Pct Recovery = 85% Analysis Date = 03/07/16 Pct Recovery = 85% Analysis Date = 03/02/16 Pct Recovery = 85% Analysis Date = 03/02/16 Pct Recovery = 85% Analysis Date = 02/26/16 Pct Recovery = 85% Analysis Date = 02/26/16 Pct Recovery = 85% Analysis Date = 02/21/16 Pct Recovery = 85% Analysis Date = 02/21/16 Pct Recovery = 85% Analysis Date = 02/17/16 Pct Recovery = 85% Analysis Date = 02/17/16 Pct Recovery = 85% Analysis Date = 02/12/16 Pct Recovery = 85% Analysis Date = 02/12/16 Pct Recovery = 85% Analysis Date = 02/07/16 Pct Recovery = 85% Analysis Date = 02/07/16 Pct Recovery = 85% Analysis Date = 02/02/16 Pct Recovery = 85% Analysis Date = 02/02/16 Pct Recovery = 85% Analysis Date = 01/28/16 Pct Recovery = 85% Analysis Date = 01/28/16 Pct Recovery = 85% Analysis Date = 01/23/16 Pct Recovery = 85% Analysis Date = 01/23/16 Pct Recovery = 85% Analysis Date = 01/19/16 Pct Recovery = 85% Analysis Date = 01/19/16 Pct Recovery = 85% Analysis Date = 01/14/16 Pct Recovery = 84% Analysis Date = 01/14/16 Pct Recovery = 84% Analysis Date = 01/09/16 Pct Recovery = 84% Analysis Date = 01/09/16 Pct Recovery = 84% Analysis Date = 01/04/16 Pct Recovery = 84% Analysis Date = 01/04/16 Pct Recovery = 84% Analysis Date = 12/30/15 Pct Recovery = 84% Analysis Date = 12/30/15 Pct Recovery = 84% Analysis Date = 12/26/15 Pct Recovery = 84% Analysis Date = 12/26/15 Pct Recovery = 84% Analysis Date = 12/21/15 Pct Recovery = 84% Analysis Date = 12/21/15 Pct Recovery = 84% Analysis Date = 12/16/15 Pct Recovery = 84% Analysis Date = 12/16/15 Pct Recovery = 84% Analysis Date = 12/11/15 Pct Recovery = 84% Analysis Date = 12/11/15 Pct Recovery = 84% Analysis Date = 12/06/15 Pct Recovery = 84% Analysis Date = 12/06/15 Pct Recovery = 84% Analysis Date = 12/01/15 Pct Recovery = 84% Analysis Date = 12/01/15 Pct Recovery = 84% Analysis Date = 11/27/15 Pct Recovery = 84% Analysis Date = 11/27/15 Pct Recovery = 84% Analysis Date = 11/22/15 Pct Recovery = 84% Analysis Date = 11/22/15 Pct Recovery = 84% Analysis Date = 11/17/15 Pct Recovery = 84% Analysis Date = 11/17/15 Pct Recovery = 84% Analysis Date = 11/12/15 Pct Recovery = 84% Analysis Date = 11/12/15 Pct Recovery = 84% Analysis Date = 11/07/15 Pct Recovery = 84% Analysis Date = 11/07/15 Pct Recovery = 84% Analysis Date = 11/03/15 Pct Recovery = 83% Analysis Date = 11/03/15 Pct Recovery = 83% Analysis Date = 10/29/15 Pct Recovery = 83% Analysis Date = 10/29/15 Pct Recovery = 83% Analysis Date = 10/24/15 Pct Recovery = 83% Analysis Date = 10/24/15 Pct Recovery = 83% Analysis Date = 10/19/15 Pct Recovery = 83% Analysis Date = 10/19/15 Pct Recovery = 83% Analysis Date = 10/14/15 Pct Recovery = 83% Analysis Date = 10/14/15 Pct Recovery = 83% Analysis Date = 10/09/15 Pct Recovery = 83% Analysis Date = 10/09/15 Pct Recovery = 83% Analysis Date = 10/05/15 Pct Recovery = 83% Analysis Date = 10/05/15 Pct Recovery = 83% Analysis Date = 09/30/15 Pct Recovery = 83% Analysis Date = 09/30/15 Pct Recovery = 83% Analysis Date = 09/25/15 Pct Recovery = 83% Analysis Date = 09/25/15 Pct Recovery = 83% Analysis Date = 09/20/15 Pct Recovery = 83% Analysis Date = 09/20/15 Pct Recovery = 83% Analysis Date = 09/15/15 Pct Recovery = 82% Analysis Date = 09/15/15 Pct Recovery = 82% Analysis Date = 09/10/15 Pct Recovery = 82% Analysis Date = 09/10/15 Pct Recovery = 82% Analysis Date = 09/06/15 Pct Recovery = 82% Analysis Date = 09/06/15 Pct Recovery = 82% Analysis Date = 09/01/15 Pct Recovery = 82% Analysis Date = 09/01/15 Pct Recovery = 82% Analysis Date = 08/27/15 Pct Recovery = 82% Analysis Date = 08/27/15 Pct Recovery = 82% Analysis Date = 08/22/15 Pct Recovery = 82% Analysis Date = 08/22/15 Pct Recovery = 82% Analysis Date = 08/17/15 Pct Recovery = 82% Analysis Date = 08/17/15 Pct Recovery = 82% Analysis Date = 08/13/15 Pct Recovery = 82% Analysis Date = 08/13/15 Pct Recovery = 82% Analysis Date = 08/08/15 Pct Recovery = 82% Analysis Date = 08/08/15 Pct Recovery = 82% Analysis Date = 08/03/15 Pct Recovery = 81% Analysis Date = 08/03/15 Pct Recovery = 81% Analysis Date = 07/29/15 Pct Recovery = 81% Analysis Date = 07/29/15 Pct Recovery = 81% Analysis Date = 07/24/15 Pct Recovery = 81% Analysis Date = 07/24/15 Pct Recovery = 81% Analysis Date = 07/19/15 Pct Recovery = 81% Analysis Date = 07/19/15 Pct Recovery = 81% Analysis Date = 07/15/15 Pct Recovery = 81% Analysis Date = 07/15/15 Pct Recovery = 81% Analysis Date = 07/10/15 Pct Recovery = 81% Analysis Date = 07/10/15 Pct Recovery = 81% Analysis Date = 07/05/15 Pct Recovery = 81% Analysis Date = 07/05/15 Pct Recovery = 81% Analysis Date = 06/30/15 Pct Recovery = 81% Analysis Date = 06/30/15 Pct Recovery = 81% Analysis Date = 06/25/15 Pct Recovery = 80% Analysis Date = 06/25/15 Pct Recovery = 80% Analysis Date = 06/21/15 Pct Recovery = 80% Analysis Date = 06/21/15 Pct Recovery = 80% Analysis Date = 06/16/15 Pct Recovery = 80% Analysis Date = 06/16/15 Pct Recovery = 80% Analysis Date = 06/11/15 Pct Recovery = 80% Analysis Date = 06/11/15 Pct Recovery = 80% Analysis Date = 06/06/15 Pct Recovery = 80% Analysis Date = 06/06/15 Pct Recovery = 80% Analysis Date = 06/01/15 Pct Recovery = 80% Analysis Date = 06/01/15 Pct Recovery = 80% Analysis Date = 05/27/15 Pct Recovery = 80% Analysis Date = 05/27/15 Pct Recovery = 80% Analysis Date = 05/23/15 Pct Recovery = 79% Analysis Date = 05/23/15 Pct Recovery = 79% Analysis Date = 05/18/15 Pct Recovery = 79% Analysis Date = 05/18/15 Pct Recovery = 79% Analysis Date = 05/13/15 Pct Recovery = 79% Analysis Date = 05/13/15 Pct Recovery = 79% Analysis Date = 05/08/15 Pct Recovery = 79% Analysis Date = 05/08/15 Pct Recovery = 79% Analysis Date = 05/03/15 Pct Recovery = 79% Analysis Date = 05/03/15 Pct Recovery = 79% Analysis Date = 04/29/15 Pct Recovery = 79% Analysis Date = 04/29/15 Pct Recovery = 79% Analysis Date = 04/24/15 Pct Recovery = 79% Analysis Date = 04/24/15 Pct Recovery = 79% Analysis Date = 04/19/15 Pct Recovery = 79% Analysis Date = 04/19/15 Pct Recovery = 79% Analysis Date = 04/14/15 Pct Recovery = 78% Analysis Date = 04/14/15 Pct Recovery = 78% Analysis Date = 04/09/15 Pct Recovery = 78% Analysis Date = 04/09/15 Pct Recovery = 78% Analysis Date = 04/04/15 Pct Recovery = 78% Analysis Date = 04/04/15 Pct Recovery = 78% Analysis Date = 03/31/15 Pct Recovery = 78% Analysis Date = 03/31/15 Pct Recovery = 78% Analysis Date = 03/26/15 Pct Recovery = 78% Analysis Date = 03/26/15 Pct Recovery = 78% Analysis Date = 03/21/15 Pct Recovery = 78% Analysis Date = 03/21/15 Pct Recovery = 78% Analysis Date = 03/16/15 Pct Recovery = 77% Analysis Date = 03/16/15 Pct Recovery = 77% Analysis Date = 03/11/15 Pct Recovery = 77% Analysis Date = 03/11/15 Pct Recovery = 77% Analysis Date = 03/07/15 Pct Recovery = 77% Analysis Date = 03/07/15 Pct Recovery = 77% Analysis Date = 03/02/15 Pct Recovery = 77% Analysis Date = 03/02/15 Pct Recovery = 77% Analysis Date = 02/25/15 Pct Recovery = 77% Analysis Date = 02/25/15 Pct Recovery = 77% Analysis Date = 02/20/15 Pct Recovery = 76% Analysis Date = 02/20/15 Pct Recovery = 76% Analysis Date = 02/15/15 Pct Recovery = 76% Analysis Date = 02/15/15 Pct Recovery = 76% Analysis Date = 02/10/15 Pct Recovery = 76% Analysis Date = 02/10/15 Pct Recovery = 76% Analysis Date = 02/06/15 Pct Recovery = 76% Analysis Date = 02/06/15 Pct Recovery = 76% Analysis Date = 02/01/15 Pct Recovery = 76% Analysis Date = 02/01/15 Pct Recovery = 76% Analysis Date = 01/27/15 Pct Recovery = 76% Analysis Date = 01/27/15 Pct Recovery = 76% Analysis Date = 01/22/15 Pct Recovery = 75% Analysis Date = 01/22/15 Pct Recovery = 75% Analysis Date = 01/17/15 Pct Recovery = 75% Analysis Date = 01/17/15 Pct Recovery = 75% Analysis Date = 01/12/15 Pct Recovery = 75% Analysis Date = 01/12/15 Pct Recovery = 75% Analysis Date = 01/08/15 Pct Recovery = 75% Analysis Date = 01/08/15 Pct Recovery = 75% Analysis Date = 01/03/15 Pct Recovery = 75% Analysis Date = 01/03/15 Pct Recovery = 75% Analysis Date = 12/29/14 Pct Recovery = 74% Analysis Date = 12/29/14 Pct Recovery = 74% Analysis Date = 12/24/14 Pct Recovery = 74% Analysis Date = 12/24/14 Pct Recovery = 74% Analysis Date = 12/19/14 Pct Recovery = 74% Analysis Date = 12/19/14 Pct Recovery = 74% Analysis Date = 12/15/14 Pct Recovery = 74% Analysis Date = 12/15/14 Pct Recovery = 74% Analysis Date = 12/10/14 Pct Recovery = 74% Analysis Date = 12/10/14 Pct Recovery = 74% Analysis Date = 12/05/14 Pct Recovery = 74% Analysis Date = 12/05/14 Pct Recovery = 74% Analysis Date = 11/30/14 Pct Recovery = 73% Analysis Date = 11/30/14 Pct Recovery = 73% Analysis Date = 11/25/14 Pct Recovery = 73% Analysis Date = 11/25/14 Pct Recovery = 73% Analysis Date = 11/20/14 Pct Recovery = 73% Analysis Date = 11/20/14 Pct Recovery = 73% Analysis Date = 11/16/14 Pct Recovery = 73% Analysis Date = 11/16/14 Pct Recovery = 73% Analysis Date = 11/11/14 Pct Recovery = 73% Analysis Date = 11/11/14 Pct Recovery = 73% Analysis Date = 11/06/14 Pct Recovery = 73% Analysis Date = 11/06/14 Pct Recovery = 73% Analysis Date = 11/01/14 Pct Recovery = 72% Analysis Date = 11/01/14 Pct Recovery = 72% Analysis Date = 10/27/14 Pct Recovery = 72% Analysis Date = 10/27/14 Pct Recovery = 72% Analysis Date = 10/23/14 Pct Recovery = 72% Analysis Date = 10/23/14 Pct Recovery = 72% Analysis Date = 10/18/14 Pct Recovery = 72% Analysis Date = 10/18/14 Pct Recovery = 72% Analysis Date = 10/13/14 Pct Recovery = 72% Analysis Date = 10/13/14 Pct Recovery = 72% Analysis Date = 10/08/14 Pct Recovery = 72% Analysis Date = 10/08/14 Pct Recovery = 72% Analysis Date = 10/03/14 Pct Recovery = 71% Analysis Date = 10/03/14 Pct Recovery = 71% Analysis Date = 09/28/14 Pct Recovery = 71% Analysis Date = 09/28/14 Pct Recovery = 71% Analysis Date = 09/24/14 Pct Recovery = 71% Analysis Date = 09/24/14 Pct Recovery = 71% Analysis Date = 09/19/14 Pct Recovery = 71% Analysis Date = 09/19/14 Pct Recovery = 71% Analysis Date = 09/14/14 Pct Recovery = 71% Analysis Date = 09/14/14 Pct Recovery = 71% Analysis Date = 09/09/14 Pct Recovery = 70% Analysis Date = 09/09/14 Pct Recovery = 70% Analysis Date = 09/04/14 Pct Recovery = 70% Analysis Date = 09/04/14 Pct Recovery = 70% Analysis Date = 08/31/14 Pct Recovery = 70% Analysis Date = 08/31/14 Pct Recovery = 70% Analysis Date = 08/26/14 Pct Recovery = 70% Analysis Date = 08/26/14 Pct Recovery = 70% Analysis Date = 08/21/14 Pct Recovery = 70% Analysis Date = 08/21/14 Pct Recovery = 70% Analysis Date = 08/16/14 Pct Recovery = 70% Analysis Date = 08/16/14 Pct Recovery = 70% Analysis Date = 08/11/14 Pct Recovery = 69% Analysis Date = 08/11/14 Pct Recovery = 69% Analysis Date = 08/06/14 Pct Recovery = 69% Analysis Date = 08/06/14 Pct Recovery = 69% Analysis Date = 08/02/14 Pct Recovery = 69% Analysis Date = 08/02/14 Pct Recovery = 69% Analysis Date = 07/28/14 Pct Recovery = 69% Analysis Date = 07/28/14 Pct Recovery = 69% Analysis Date = 07/23/14 Pct Recovery = 69% Analysis Date = 07/23/14 Pct Recovery = 69% Analysis Date = 07/18/14 Pct Recovery = 69% Analysis Date = 07/18/14 Pct Recovery = 69% Analysis Date = 07/13/14 Pct Recovery = 68% Analysis Date = 07/13/14 Pct Recovery = 68% Analysis Date = 07/09/14 Pct Recovery = 68% Analysis Date = 07/09/14 Pct Recovery = 68% Analysis Date = 07/04/14 Pct Recovery = 68% Analysis Date = 07/04/14 Pct Recovery = 68% Analysis Date = 06/29/14 Pct Recovery = 68% Analysis Date = 06/29/14 Pct Recovery = 68% Analysis Date = 06/24/14 Pct Recovery = 68% Analysis Date = 06/24/14 Pct Recovery = 68% Analysis Date = 06/19/14 Pct Recovery = 67% Analysis Date = 06/19/14 Pct Recovery = 67% Analysis Date = 06/14/14 Pct Recovery = 67% Analysis Date = 06/14/14 Pct Recovery = 67% Analysis Date = 06/10/14 Pct Recovery = 67% Analysis Date = 06/10/14 Pct Recovery = 67% Analysis Date = 06/05/14 Pct Recovery = 67% Analysis Date = 06/05/14 Pct Recovery = 67% Analysis Date = 05/31/14 Pct Recovery = 67% Analysis Date = 05/31/14 Pct Recovery = 67% Analysis Date = 05/26/14 Pct Recovery = 66% Analysis Date = 05/26/14 Pct Recovery = 66% Analysis Date = 05/21/14 Pct Recovery = 66% Analysis Date = 05/21/14 Pct Recovery = 66% Analysis Date = 05/17/14 Pct Recovery = 66% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
NADALOL

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 2 76% 18% 76% 19%
>= Reporting Level 74 81% 17% 77% 13%
Total 76 81% 17% 77% 13%

Sample Statistics
NADALOL

Characteristic N % % Basis
Plotted 76 100% Spiked
Estimated Values 8 11% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 76 .  
False Negatives 0 0% 0 out of 76
Not Spiked 39 .  
False Positives 0 0% 0 out of 39

BQS OBSP Determination:
NEVIRAPINE
METHOD: 2440 , TESTIDCODE: 68017LCM56
Open Data Set

Analysis Date = 02/23/16 SpikeMix = Abs 050115: 80 µl & ERA 0406-15-08: 80 µl Pct Recovery = 79% Analysis Date = 11/05/15 SpikeMix = ERA 0406-15-08: 80 µl & Abs 052215: 80 µl Pct Recovery = 82% Analysis Date = 11/24/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 87% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 80 µl & Abs 051315: 80 µl Pct Recovery = 82% Analysis Date = 10/01/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 75% Analysis Date = 09/24/16 SpikeMix = Crescent EN160610015: 80 µl & Abs 061416: 80 µl Pct Recovery = 82% Analysis Date = 09/24/16 SpikeMix = Abs 061416: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 78% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 72% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 72% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 70% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 68% Analysis Date = 05/07/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 120% Analysis Date = 04/29/15 SpikeMix = ERA 0319-14-05: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 112% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 97% Analysis Date = 01/16/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 94% Analysis Date = 12/07/14 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 93% Analysis Date = 12/06/14 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 84% Analysis Date = 08/28/14 SpikeMix = ERA 0319-14-04: 60 µl & ERA 0319-14-05: 60 µl Pct Recovery = 70% Analysis Date = 07/26/14 SpikeMix = ERA 0319-14-05: 60 µl & ERA 0318-14-02: 60 µl Pct Recovery = 87% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-04: 15 µl & Abs 041814: 15 µl Pct Recovery = 73% Analysis Date = 02/06/15 SpikeMix = Abs 041814: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 77% Analysis Date = 07/12/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 64% Analysis Date = 06/22/14 SpikeMix = Abs 041814: 60 µl & Abs 041614: 60 µl Pct Recovery = 83% Analysis Date = 05/21/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 54% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-08: 40 µl & Abs 052215: 40 µl Pct Recovery = 72% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 74% Analysis Date = 11/04/15 SpikeMix = ERA 0406-15-07A: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 72% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-08: 40 µl & ERA 0406-15-09: 40 µl Pct Recovery = 69% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 89% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 71% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-07A: 40 µl & Abs 051315: 40 µl Pct Recovery = 76% Analysis Date = 07/31/15 SpikeMix = Abs 051315: 40 µl & Abs 052215: 40 µl Pct Recovery = 61% Analysis Date = 07/30/15 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 78% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 79% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 83% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 75% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 70% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 70% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 70% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 85% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 68% Analysis Date = 11/04/14 SpikeMix = Abs 041714: 8 µl & ERA 0319-14-05: 8 µl Pct Recovery = 83% Analysis Date = 10/24/14 SpikeMix = ERA 0319-14-05: 8 µl & Abs 041614: 8 µl Pct Recovery = 92% Analysis Date = 04/10/15 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 85% Analysis Date = 11/04/14 SpikeMix = Abs 041814: 8 µl & ERA 0318-14-02: 8 µl Pct Recovery = 76% Analysis Date = 10/11/14 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 63% Analysis Date = 08/30/14 SpikeMix = ERA 0318-14-02: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 88% Analysis Date = 08/16/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 47% Analysis Date = 07/13/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 76% Analysis Date = 10/10/14 SpikeMix = Abs 041714: 30 µl & Abs 041814: 30 µl Pct Recovery = 75% Analysis Date = 10/10/14 SpikeMix = Abs 041814: 30 µl & ERA 0318-14-02: 30 µl Pct Recovery = 65% Analysis Date = 07/13/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 64% Analysis Date = 05/30/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 66% Analysis Date = 04/27/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 108% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 73% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-08: 20 µl & ERA 0406-15-09: 20 µl Pct Recovery = 71% Analysis Date = 11/25/15 SpikeMix = Abs 050115: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 70% Analysis Date = 09/15/15 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 69% Analysis Date = 09/09/15 SpikeMix = ERA 0406-15-08: 20 µl & Abs 052215: 20 µl Pct Recovery = 89% Analysis Date = 02/23/16 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 79% Analysis Date = 08/11/15 SpikeMix = Abs 050115: 20 µl & Abs 051315: 20 µl Pct Recovery = 68% Analysis Date = 06/26/15 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 78% Analysis Date = 06/09/15 SpikeMix = Abs 051315: 20 µl & Abs 050115: 20 µl Pct Recovery = 86% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 85% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 84% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 78% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 77% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 73% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 72% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 109% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 106% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 82% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 85% Analysis Date = 04/09/16 SpikeMix = Abs 051315: 10 µl & ERA 0406-15-09: 10 µl Pct Recovery = 60% Analysis Date = 04/09/16 SpikeMix = Abs 051315: 10 µl & ERA 0406-15-09: 10 µl Pct Recovery = 71% Analysis Date = 01/18/17 Pct Recovery = 83% Analysis Date = 01/14/17 Pct Recovery = 83% Analysis Date = 01/14/17 Pct Recovery = 83% Analysis Date = 01/09/17 Pct Recovery = 83% Analysis Date = 01/09/17 Pct Recovery = 83% Analysis Date = 01/04/17 Pct Recovery = 83% Analysis Date = 01/04/17 Pct Recovery = 83% Analysis Date = 12/30/16 Pct Recovery = 83% Analysis Date = 12/30/16 Pct Recovery = 83% Analysis Date = 12/25/16 Pct Recovery = 83% Analysis Date = 12/25/16 Pct Recovery = 83% Analysis Date = 12/20/16 Pct Recovery = 82% Analysis Date = 12/20/16 Pct Recovery = 82% Analysis Date = 12/15/16 Pct Recovery = 82% Analysis Date = 12/15/16 Pct Recovery = 82% Analysis Date = 12/11/16 Pct Recovery = 82% Analysis Date = 12/11/16 Pct Recovery = 82% Analysis Date = 12/06/16 Pct Recovery = 82% Analysis Date = 12/06/16 Pct Recovery = 82% Analysis Date = 12/01/16 Pct Recovery = 82% Analysis Date = 12/01/16 Pct Recovery = 82% Analysis Date = 11/26/16 Pct Recovery = 82% Analysis Date = 11/26/16 Pct Recovery = 82% Analysis Date = 11/21/16 Pct Recovery = 81% Analysis Date = 11/21/16 Pct Recovery = 81% Analysis Date = 11/16/16 Pct Recovery = 81% Analysis Date = 11/16/16 Pct Recovery = 81% Analysis Date = 11/11/16 Pct Recovery = 81% Analysis Date = 11/11/16 Pct Recovery = 81% Analysis Date = 11/06/16 Pct Recovery = 81% Analysis Date = 11/06/16 Pct Recovery = 81% Analysis Date = 11/02/16 Pct Recovery = 81% Analysis Date = 11/02/16 Pct Recovery = 81% Analysis Date = 10/28/16 Pct Recovery = 81% Analysis Date = 10/28/16 Pct Recovery = 81% Analysis Date = 10/23/16 Pct Recovery = 80% Analysis Date = 10/23/16 Pct Recovery = 80% Analysis Date = 10/18/16 Pct Recovery = 80% Analysis Date = 10/18/16 Pct Recovery = 80% Analysis Date = 10/13/16 Pct Recovery = 80% Analysis Date = 10/13/16 Pct Recovery = 80% Analysis Date = 10/08/16 Pct Recovery = 80% Analysis Date = 10/08/16 Pct Recovery = 80% Analysis Date = 10/03/16 Pct Recovery = 80% Analysis Date = 10/03/16 Pct Recovery = 80% Analysis Date = 09/28/16 Pct Recovery = 80% Analysis Date = 09/28/16 Pct Recovery = 80% Analysis Date = 09/24/16 Pct Recovery = 80% Analysis Date = 09/24/16 Pct Recovery = 80% Analysis Date = 09/19/16 Pct Recovery = 79% Analysis Date = 09/19/16 Pct Recovery = 79% Analysis Date = 09/14/16 Pct Recovery = 79% Analysis Date = 09/14/16 Pct Recovery = 79% Analysis Date = 09/09/16 Pct Recovery = 79% Analysis Date = 09/09/16 Pct Recovery = 79% Analysis Date = 09/04/16 Pct Recovery = 79% Analysis Date = 09/04/16 Pct Recovery = 79% Analysis Date = 08/30/16 Pct Recovery = 79% Analysis Date = 08/30/16 Pct Recovery = 79% Analysis Date = 08/25/16 Pct Recovery = 79% Analysis Date = 08/25/16 Pct Recovery = 79% Analysis Date = 08/21/16 Pct Recovery = 79% Analysis Date = 08/21/16 Pct Recovery = 79% Analysis Date = 08/16/16 Pct Recovery = 78% Analysis Date = 08/16/16 Pct Recovery = 78% Analysis Date = 08/11/16 Pct Recovery = 78% Analysis Date = 08/11/16 Pct Recovery = 78% Analysis Date = 08/06/16 Pct Recovery = 78% Analysis Date = 08/06/16 Pct Recovery = 78% Analysis Date = 08/01/16 Pct Recovery = 78% Analysis Date = 08/01/16 Pct Recovery = 78% Analysis Date = 07/27/16 Pct Recovery = 78% Analysis Date = 07/27/16 Pct Recovery = 78% Analysis Date = 07/22/16 Pct Recovery = 78% Analysis Date = 07/22/16 Pct Recovery = 78% Analysis Date = 07/17/16 Pct Recovery = 78% Analysis Date = 07/17/16 Pct Recovery = 78% Analysis Date = 07/13/16 Pct Recovery = 78% Analysis Date = 07/13/16 Pct Recovery = 78% Analysis Date = 07/08/16 Pct Recovery = 78% Analysis Date = 07/08/16 Pct Recovery = 78% Analysis Date = 07/03/16 Pct Recovery = 78% Analysis Date = 07/03/16 Pct Recovery = 78% Analysis Date = 06/28/16 Pct Recovery = 78% Analysis Date = 06/28/16 Pct Recovery = 78% Analysis Date = 06/23/16 Pct Recovery = 77% Analysis Date = 06/23/16 Pct Recovery = 77% Analysis Date = 06/18/16 Pct Recovery = 77% Analysis Date = 06/18/16 Pct Recovery = 77% Analysis Date = 06/13/16 Pct Recovery = 77% Analysis Date = 06/13/16 Pct Recovery = 77% Analysis Date = 06/08/16 Pct Recovery = 77% Analysis Date = 06/08/16 Pct Recovery = 77% Analysis Date = 06/04/16 Pct Recovery = 77% Analysis Date = 06/04/16 Pct Recovery = 77% Analysis Date = 05/30/16 Pct Recovery = 77% Analysis Date = 05/30/16 Pct Recovery = 77% Analysis Date = 05/25/16 Pct Recovery = 77% Analysis Date = 05/25/16 Pct Recovery = 77% Analysis Date = 05/20/16 Pct Recovery = 77% Analysis Date = 05/20/16 Pct Recovery = 77% Analysis Date = 05/15/16 Pct Recovery = 77% Analysis Date = 05/15/16 Pct Recovery = 77% Analysis Date = 05/10/16 Pct Recovery = 77% Analysis Date = 05/10/16 Pct Recovery = 77% Analysis Date = 05/05/16 Pct Recovery = 77% Analysis Date = 05/05/16 Pct Recovery = 77% Analysis Date = 05/01/16 Pct Recovery = 76% Analysis Date = 05/01/16 Pct Recovery = 76% Analysis Date = 04/26/16 Pct Recovery = 76% Analysis Date = 04/26/16 Pct Recovery = 76% Analysis Date = 04/21/16 Pct Recovery = 76% Analysis Date = 04/21/16 Pct Recovery = 76% Analysis Date = 04/16/16 Pct Recovery = 76% Analysis Date = 04/16/16 Pct Recovery = 76% Analysis Date = 04/11/16 Pct Recovery = 76% Analysis Date = 04/11/16 Pct Recovery = 76% Analysis Date = 04/06/16 Pct Recovery = 76% Analysis Date = 04/06/16 Pct Recovery = 76% Analysis Date = 04/01/16 Pct Recovery = 76% Analysis Date = 04/01/16 Pct Recovery = 76% Analysis Date = 03/27/16 Pct Recovery = 76% Analysis Date = 03/27/16 Pct Recovery = 76% Analysis Date = 03/23/16 Pct Recovery = 76% Analysis Date = 03/23/16 Pct Recovery = 76% Analysis Date = 03/18/16 Pct Recovery = 76% Analysis Date = 03/18/16 Pct Recovery = 76% Analysis Date = 03/13/16 Pct Recovery = 76% Analysis Date = 03/13/16 Pct Recovery = 76% Analysis Date = 03/08/16 Pct Recovery = 76% Analysis Date = 03/08/16 Pct Recovery = 76% Analysis Date = 03/03/16 Pct Recovery = 76% Analysis Date = 03/03/16 Pct Recovery = 76% Analysis Date = 02/27/16 Pct Recovery = 76% Analysis Date = 02/27/16 Pct Recovery = 76% Analysis Date = 02/22/16 Pct Recovery = 76% Analysis Date = 02/22/16 Pct Recovery = 76% Analysis Date = 02/17/16 Pct Recovery = 76% Analysis Date = 02/17/16 Pct Recovery = 76% Analysis Date = 02/13/16 Pct Recovery = 76% Analysis Date = 02/13/16 Pct Recovery = 76% Analysis Date = 02/08/16 Pct Recovery = 76% Analysis Date = 02/08/16 Pct Recovery = 76% Analysis Date = 02/03/16 Pct Recovery = 76% Analysis Date = 02/03/16 Pct Recovery = 76% Analysis Date = 01/29/16 Pct Recovery = 76% Analysis Date = 01/29/16 Pct Recovery = 76% Analysis Date = 01/24/16 Pct Recovery = 76% Analysis Date = 01/24/16 Pct Recovery = 76% Analysis Date = 01/19/16 Pct Recovery = 77% Analysis Date = 01/19/16 Pct Recovery = 77% Analysis Date = 01/14/16 Pct Recovery = 77% Analysis Date = 01/14/16 Pct Recovery = 77% Analysis Date = 01/10/16 Pct Recovery = 77% Analysis Date = 01/10/16 Pct Recovery = 77% Analysis Date = 01/05/16 Pct Recovery = 77% Analysis Date = 01/05/16 Pct Recovery = 77% Analysis Date = 12/31/15 Pct Recovery = 77% Analysis Date = 12/31/15 Pct Recovery = 77% Analysis Date = 12/26/15 Pct Recovery = 77% Analysis Date = 12/26/15 Pct Recovery = 77% Analysis Date = 12/21/15 Pct Recovery = 77% Analysis Date = 12/21/15 Pct Recovery = 77% Analysis Date = 12/16/15 Pct Recovery = 77% Analysis Date = 12/16/15 Pct Recovery = 77% Analysis Date = 12/11/15 Pct Recovery = 77% Analysis Date = 12/11/15 Pct Recovery = 77% Analysis Date = 12/06/15 Pct Recovery = 77% Analysis Date = 12/06/15 Pct Recovery = 77% Analysis Date = 12/02/15 Pct Recovery = 77% Analysis Date = 12/02/15 Pct Recovery = 77% Analysis Date = 11/27/15 Pct Recovery = 77% Analysis Date = 11/27/15 Pct Recovery = 77% Analysis Date = 11/22/15 Pct Recovery = 77% Analysis Date = 11/22/15 Pct Recovery = 77% Analysis Date = 11/17/15 Pct Recovery = 78% Analysis Date = 11/17/15 Pct Recovery = 78% Analysis Date = 11/12/15 Pct Recovery = 78% Analysis Date = 11/12/15 Pct Recovery = 78% Analysis Date = 11/07/15 Pct Recovery = 78% Analysis Date = 11/07/15 Pct Recovery = 78% Analysis Date = 11/02/15 Pct Recovery = 78% Analysis Date = 11/02/15 Pct Recovery = 78% Analysis Date = 10/28/15 Pct Recovery = 78% Analysis Date = 10/28/15 Pct Recovery = 78% Analysis Date = 10/24/15 Pct Recovery = 78% Analysis Date = 10/24/15 Pct Recovery = 78% Analysis Date = 10/19/15 Pct Recovery = 79% Analysis Date = 10/19/15 Pct Recovery = 79% Analysis Date = 10/14/15 Pct Recovery = 79% Analysis Date = 10/14/15 Pct Recovery = 79% Analysis Date = 10/09/15 Pct Recovery = 79% Analysis Date = 10/09/15 Pct Recovery = 79% Analysis Date = 10/04/15 Pct Recovery = 79% Analysis Date = 10/04/15 Pct Recovery = 79% Analysis Date = 09/29/15 Pct Recovery = 79% Analysis Date = 09/29/15 Pct Recovery = 79% Analysis Date = 09/24/15 Pct Recovery = 79% Analysis Date = 09/24/15 Pct Recovery = 79% Analysis Date = 09/19/15 Pct Recovery = 80% Analysis Date = 09/19/15 Pct Recovery = 80% Analysis Date = 09/15/15 Pct Recovery = 80% Analysis Date = 09/15/15 Pct Recovery = 80% Analysis Date = 09/10/15 Pct Recovery = 80% Analysis Date = 09/10/15 Pct Recovery = 80% Analysis Date = 09/05/15 Pct Recovery = 80% Analysis Date = 09/05/15 Pct Recovery = 80% Analysis Date = 08/31/15 Pct Recovery = 80% Analysis Date = 08/31/15 Pct Recovery = 80% Analysis Date = 08/26/15 Pct Recovery = 80% Analysis Date = 08/26/15 Pct Recovery = 80% Analysis Date = 08/21/15 Pct Recovery = 81% Analysis Date = 08/21/15 Pct Recovery = 81% Analysis Date = 08/16/15 Pct Recovery = 81% Analysis Date = 08/16/15 Pct Recovery = 81% Analysis Date = 08/12/15 Pct Recovery = 81% Analysis Date = 08/12/15 Pct Recovery = 81% Analysis Date = 08/07/15 Pct Recovery = 81% Analysis Date = 08/07/15 Pct Recovery = 81% Analysis Date = 08/02/15 Pct Recovery = 81% Analysis Date = 08/02/15 Pct Recovery = 81% Analysis Date = 07/28/15 Pct Recovery = 81% Analysis Date = 07/28/15 Pct Recovery = 81% Analysis Date = 07/23/15 Pct Recovery = 81% Analysis Date = 07/23/15 Pct Recovery = 81% Analysis Date = 07/18/15 Pct Recovery = 81% Analysis Date = 07/18/15 Pct Recovery = 81% Analysis Date = 07/13/15 Pct Recovery = 81% Analysis Date = 07/13/15 Pct Recovery = 81% Analysis Date = 07/08/15 Pct Recovery = 81% Analysis Date = 07/08/15 Pct Recovery = 81% Analysis Date = 07/04/15 Pct Recovery = 81% Analysis Date = 07/04/15 Pct Recovery = 81% Analysis Date = 06/29/15 Pct Recovery = 81% Analysis Date = 06/29/15 Pct Recovery = 81% Analysis Date = 06/24/15 Pct Recovery = 81% Analysis Date = 06/24/15 Pct Recovery = 81% Analysis Date = 06/19/15 Pct Recovery = 81% Analysis Date = 06/19/15 Pct Recovery = 81% Analysis Date = 06/14/15 Pct Recovery = 82% Analysis Date = 06/14/15 Pct Recovery = 82% Analysis Date = 06/09/15 Pct Recovery = 82% Analysis Date = 06/09/15 Pct Recovery = 82% Analysis Date = 06/04/15 Pct Recovery = 82% Analysis Date = 06/04/15 Pct Recovery = 82% Analysis Date = 05/30/15 Pct Recovery = 82% Analysis Date = 05/30/15 Pct Recovery = 82% Analysis Date = 05/26/15 Pct Recovery = 82% Analysis Date = 05/26/15 Pct Recovery = 82% Analysis Date = 05/21/15 Pct Recovery = 82% Analysis Date = 05/21/15 Pct Recovery = 82% Analysis Date = 05/16/15 Pct Recovery = 82% Analysis Date = 05/16/15 Pct Recovery = 82% Analysis Date = 05/11/15 Pct Recovery = 82% Analysis Date = 05/11/15 Pct Recovery = 82% Analysis Date = 05/06/15 Pct Recovery = 82% Analysis Date = 05/06/15 Pct Recovery = 82% Analysis Date = 05/01/15 Pct Recovery = 82% Analysis Date = 05/01/15 Pct Recovery = 82% Analysis Date = 04/26/15 Pct Recovery = 82% Analysis Date = 04/26/15 Pct Recovery = 82% Analysis Date = 04/22/15 Pct Recovery = 82% Analysis Date = 04/22/15 Pct Recovery = 82% Analysis Date = 04/17/15 Pct Recovery = 82% Analysis Date = 04/17/15 Pct Recovery = 82% Analysis Date = 04/12/15 Pct Recovery = 81% Analysis Date = 04/12/15 Pct Recovery = 81% Analysis Date = 04/07/15 Pct Recovery = 81% Analysis Date = 04/07/15 Pct Recovery = 81% Analysis Date = 04/02/15 Pct Recovery = 81% Analysis Date = 04/02/15 Pct Recovery = 81% Analysis Date = 03/28/15 Pct Recovery = 81% Analysis Date = 03/28/15 Pct Recovery = 81% Analysis Date = 03/23/15 Pct Recovery = 81% Analysis Date = 03/23/15 Pct Recovery = 81% Analysis Date = 03/18/15 Pct Recovery = 81% Analysis Date = 03/18/15 Pct Recovery = 81% Analysis Date = 03/14/15 Pct Recovery = 81% Analysis Date = 03/14/15 Pct Recovery = 81% Analysis Date = 03/09/15 Pct Recovery = 81% Analysis Date = 03/09/15 Pct Recovery = 81% Analysis Date = 03/04/15 Pct Recovery = 81% Analysis Date = 03/04/15 Pct Recovery = 81% Analysis Date = 02/27/15 Pct Recovery = 80% Analysis Date = 02/27/15 Pct Recovery = 80% Analysis Date = 02/22/15 Pct Recovery = 80% Analysis Date = 02/22/15 Pct Recovery = 80% Analysis Date = 02/17/15 Pct Recovery = 80% Analysis Date = 02/17/15 Pct Recovery = 80% Analysis Date = 02/12/15 Pct Recovery = 80% Analysis Date = 02/12/15 Pct Recovery = 80% Analysis Date = 02/07/15 Pct Recovery = 80% Analysis Date = 02/07/15 Pct Recovery = 80% Analysis Date = 02/03/15 Pct Recovery = 80% Analysis Date = 02/03/15 Pct Recovery = 80% Analysis Date = 01/29/15 Pct Recovery = 80% Analysis Date = 01/29/15 Pct Recovery = 80% Analysis Date = 01/24/15 Pct Recovery = 80% Analysis Date = 01/24/15 Pct Recovery = 80% Analysis Date = 01/19/15 Pct Recovery = 80% Analysis Date = 01/19/15 Pct Recovery = 80% Analysis Date = 01/14/15 Pct Recovery = 79% Analysis Date = 01/14/15 Pct Recovery = 79% Analysis Date = 01/09/15 Pct Recovery = 79% Analysis Date = 01/09/15 Pct Recovery = 79% Analysis Date = 01/04/15 Pct Recovery = 79% Analysis Date = 01/04/15 Pct Recovery = 79% Analysis Date = 12/31/14 Pct Recovery = 79% Analysis Date = 12/31/14 Pct Recovery = 79% Analysis Date = 12/26/14 Pct Recovery = 79% Analysis Date = 12/26/14 Pct Recovery = 79% Analysis Date = 12/21/14 Pct Recovery = 79% Analysis Date = 12/21/14 Pct Recovery = 79% Analysis Date = 12/16/14 Pct Recovery = 78% Analysis Date = 12/16/14 Pct Recovery = 78% Analysis Date = 12/11/14 Pct Recovery = 78% Analysis Date = 12/11/14 Pct Recovery = 78% Analysis Date = 12/06/14 Pct Recovery = 78% Analysis Date = 12/06/14 Pct Recovery = 78% Analysis Date = 12/01/14 Pct Recovery = 78% Analysis Date = 12/01/14 Pct Recovery = 78% Analysis Date = 11/26/14 Pct Recovery = 78% Analysis Date = 11/26/14 Pct Recovery = 78% Analysis Date = 11/22/14 Pct Recovery = 78% Analysis Date = 11/22/14 Pct Recovery = 78% Analysis Date = 11/17/14 Pct Recovery = 77% Analysis Date = 11/17/14 Pct Recovery = 77% Analysis Date = 11/12/14 Pct Recovery = 77% Analysis Date = 11/12/14 Pct Recovery = 77% Analysis Date = 11/07/14 Pct Recovery = 77% Analysis Date = 11/07/14 Pct Recovery = 77% Analysis Date = 11/02/14 Pct Recovery = 77% Analysis Date = 11/02/14 Pct Recovery = 77% Analysis Date = 10/28/14 Pct Recovery = 77% Analysis Date = 10/28/14 Pct Recovery = 77% Analysis Date = 10/23/14 Pct Recovery = 77% Analysis Date = 10/23/14 Pct Recovery = 77% Analysis Date = 10/18/14 Pct Recovery = 76% Analysis Date = 10/18/14 Pct Recovery = 76% Analysis Date = 10/14/14 Pct Recovery = 76% Analysis Date = 10/14/14 Pct Recovery = 76% Analysis Date = 10/09/14 Pct Recovery = 76% Analysis Date = 10/09/14 Pct Recovery = 76% Analysis Date = 10/04/14 Pct Recovery = 76% Analysis Date = 10/04/14 Pct Recovery = 76% Analysis Date = 09/29/14 Pct Recovery = 76% Analysis Date = 09/29/14 Pct Recovery = 76% Analysis Date = 09/24/14 Pct Recovery = 76% Analysis Date = 09/24/14 Pct Recovery = 76% Analysis Date = 09/19/14 Pct Recovery = 75% Analysis Date = 09/19/14 Pct Recovery = 75% Analysis Date = 09/14/14 Pct Recovery = 75% Analysis Date = 09/14/14 Pct Recovery = 75% Analysis Date = 09/10/14 Pct Recovery = 75% Analysis Date = 09/10/14 Pct Recovery = 75% Analysis Date = 09/05/14 Pct Recovery = 75% Analysis Date = 09/05/14 Pct Recovery = 75% Analysis Date = 08/31/14 Pct Recovery = 75% Analysis Date = 08/31/14 Pct Recovery = 75% Analysis Date = 08/26/14 Pct Recovery = 75% Analysis Date = 08/26/14 Pct Recovery = 75% Analysis Date = 08/21/14 Pct Recovery = 74% Analysis Date = 08/21/14 Pct Recovery = 74% Analysis Date = 08/16/14 Pct Recovery = 74% Analysis Date = 08/16/14 Pct Recovery = 74% Analysis Date = 08/11/14 Pct Recovery = 74% Analysis Date = 08/11/14 Pct Recovery = 74% Analysis Date = 08/06/14 Pct Recovery = 74% Analysis Date = 08/06/14 Pct Recovery = 74% Analysis Date = 08/02/14 Pct Recovery = 73% Analysis Date = 08/02/14 Pct Recovery = 73% Analysis Date = 07/28/14 Pct Recovery = 73% Analysis Date = 07/28/14 Pct Recovery = 73% Analysis Date = 07/23/14 Pct Recovery = 73% Analysis Date = 07/23/14 Pct Recovery = 73% Analysis Date = 07/18/14 Pct Recovery = 73% Analysis Date = 07/18/14 Pct Recovery = 73% Analysis Date = 07/13/14 Pct Recovery = 73% Analysis Date = 07/13/14 Pct Recovery = 73% Analysis Date = 07/08/14 Pct Recovery = 72% Analysis Date = 07/08/14 Pct Recovery = 72% Analysis Date = 07/03/14 Pct Recovery = 72% Analysis Date = 07/03/14 Pct Recovery = 72% Analysis Date = 06/28/14 Pct Recovery = 72% Analysis Date = 06/28/14 Pct Recovery = 72% Analysis Date = 06/24/14 Pct Recovery = 72% Analysis Date = 06/24/14 Pct Recovery = 72% Analysis Date = 06/19/14 Pct Recovery = 71% Analysis Date = 06/19/14 Pct Recovery = 71% Analysis Date = 06/14/14 Pct Recovery = 71% Analysis Date = 06/14/14 Pct Recovery = 71% Analysis Date = 06/09/14 Pct Recovery = 71% Analysis Date = 06/09/14 Pct Recovery = 71% Analysis Date = 06/04/14 Pct Recovery = 71% Analysis Date = 06/04/14 Pct Recovery = 71% Analysis Date = 05/30/14 Pct Recovery = 71% Analysis Date = 05/30/14 Pct Recovery = 71% Analysis Date = 05/25/14 Pct Recovery = 70% Analysis Date = 05/25/14 Pct Recovery = 70% Analysis Date = 05/21/14 Pct Recovery = 70% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
NEVIRAPINE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 12 82% 14% 80% 9%
>= Reporting Level 63 78% 13% 76% 11%
Total 75 78% 13% 76% 11%

Sample Statistics
NEVIRAPINE

Characteristic N % % Basis
Plotted 75 100% Spiked
Estimated Values 6 8% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 75 .  
False Negatives 0 0% 0 out of 75
Not Spiked 40 .  
False Positives 0 0% 0 out of 40

BQS OBSP Determination:
NICOTINE
METHOD: 2440 , TESTIDCODE: 67493LCM56
Open Data Set

Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 28% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 27% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 80 µl & ERA 0406-15-08: 80 µl Pct Recovery = 60% Analysis Date = 11/05/15 SpikeMix = ERA 0406-15-08: 80 µl & Abs 052215: 80 µl Pct Recovery = 62% Analysis Date = 11/24/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 62% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 80 µl & Abs 051315: 80 µl Pct Recovery = 55% Analysis Date = 10/01/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 41% Analysis Date = 09/24/16 SpikeMix = Crescent EN160610015: 80 µl & Abs 061416: 80 µl Pct Recovery = 54% Analysis Date = 09/24/16 SpikeMix = Abs 061416: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 42% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 17% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 29% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 37% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 33% Analysis Date = 11/18/16 SpikeMix = ERA 04281604: 80 µl & ERA 04281603: 80 µl Pct Recovery = 47% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & ERA 04281604: 80 µl Pct Recovery = 69% Analysis Date = 05/07/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 34% Analysis Date = 03/11/15 SpikeMix = ERA 0318-14-02: 15 µl & Abs 041714: 15 µl Pct Recovery = 47% Analysis Date = 01/16/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 53% Analysis Date = 12/06/14 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 77% Analysis Date = 08/21/14 SpikeMix = ERA 0318-14-02: 60 µl & Abs 041714: 60 µl Pct Recovery = 56% Analysis Date = 07/12/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 22% Analysis Date = 06/11/14 SpikeMix = Abs 041614: 60 µl & Abs 041714: 60 µl Pct Recovery = 54% Analysis Date = 05/21/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 75% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-04: 15 µl & Abs 041814: 15 µl Pct Recovery = 64% Analysis Date = 12/06/14 SpikeMix = ERA 0318-14-02: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 77% Analysis Date = 10/25/14 SpikeMix = Abs 041614: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 32% Analysis Date = 10/11/14 SpikeMix = ERA 0318-14-02: 60 µl & ERA 0319-14-04: 60 µl Pct Recovery = 79% Analysis Date = 08/28/14 SpikeMix = ERA 0319-14-04: 60 µl & ERA 0319-14-05: 60 µl Pct Recovery = 53% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-08: 40 µl & Abs 052215: 40 µl Pct Recovery = 36% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 35% Analysis Date = 11/04/15 SpikeMix = ERA 0406-15-07A: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 31% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-08: 40 µl & ERA 0406-15-09: 40 µl Pct Recovery = 65% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 13% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 16% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-07A: 40 µl & Abs 051315: 40 µl Pct Recovery = 19% Analysis Date = 07/30/15 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 41% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 44% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 40% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 42% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 33% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 85% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 58% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 62% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 62% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 33% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 37% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 26% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 26% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 52% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 34% Analysis Date = 11/04/14 SpikeMix = Abs 041714: 8 µl & ERA 0319-14-05: 8 µl Pct Recovery = 31% Analysis Date = 04/30/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 139% Analysis Date = 04/10/15 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 44% Analysis Date = 02/10/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 46% Analysis Date = 12/07/14 SpikeMix = ERA 0318-14-02: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 109% Analysis Date = 10/11/14 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 31% Analysis Date = 10/10/14 SpikeMix = Abs 041714: 30 µl & Abs 041814: 30 µl Pct Recovery = 70% Analysis Date = 07/20/14 SpikeMix = ERA 0318-14-02: 30 µl & Abs 041714: 30 µl Pct Recovery = 43% Analysis Date = 06/28/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 35% Analysis Date = 05/17/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 72% Analysis Date = 09/12/14 SpikeMix = Abs 041614: 30 µl & ERA 0319-14-04: 30 µl Pct Recovery = 66% Analysis Date = 08/16/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 66% Analysis Date = 07/13/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 61% Analysis Date = 04/23/14 SpikeMix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.2: 20 µl Pct Recovery = 55% Analysis Date = 04/27/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 61% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-08: 20 µl & ERA 0406-15-09: 20 µl Pct Recovery = 21% Analysis Date = 11/25/15 SpikeMix = Abs 050115: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 139% Analysis Date = 09/15/15 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 93% Analysis Date = 09/09/15 SpikeMix = ERA 0406-15-08: 20 µl & Abs 052215: 20 µl Pct Recovery = 117% Analysis Date = 08/11/15 SpikeMix = Abs 050115: 20 µl & Abs 051315: 20 µl Pct Recovery = 24% Analysis Date = 06/26/15 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 57% Analysis Date = 06/09/15 SpikeMix = Abs 051315: 20 µl & Abs 050115: 20 µl Pct Recovery = 68% Analysis Date = 01/04/17 Pct Recovery = 40% Analysis Date = 12/31/16 Pct Recovery = 40% Analysis Date = 12/31/16 Pct Recovery = 40% Analysis Date = 12/26/16 Pct Recovery = 40% Analysis Date = 12/26/16 Pct Recovery = 40% Analysis Date = 12/21/16 Pct Recovery = 40% Analysis Date = 12/21/16 Pct Recovery = 40% Analysis Date = 12/16/16 Pct Recovery = 40% Analysis Date = 12/16/16 Pct Recovery = 40% Analysis Date = 12/11/16 Pct Recovery = 41% Analysis Date = 12/11/16 Pct Recovery = 41% Analysis Date = 12/06/16 Pct Recovery = 41% Analysis Date = 12/06/16 Pct Recovery = 41% Analysis Date = 12/01/16 Pct Recovery = 41% Analysis Date = 12/01/16 Pct Recovery = 41% Analysis Date = 11/26/16 Pct Recovery = 41% Analysis Date = 11/26/16 Pct Recovery = 41% Analysis Date = 11/21/16 Pct Recovery = 41% Analysis Date = 11/21/16 Pct Recovery = 41% Analysis Date = 11/16/16 Pct Recovery = 41% Analysis Date = 11/16/16 Pct Recovery = 41% Analysis Date = 11/11/16 Pct Recovery = 41% Analysis Date = 11/11/16 Pct Recovery = 41% Analysis Date = 11/06/16 Pct Recovery = 41% Analysis Date = 11/06/16 Pct Recovery = 41% Analysis Date = 11/01/16 Pct Recovery = 41% Analysis Date = 11/01/16 Pct Recovery = 41% Analysis Date = 10/27/16 Pct Recovery = 41% Analysis Date = 10/27/16 Pct Recovery = 41% Analysis Date = 10/22/16 Pct Recovery = 41% Analysis Date = 10/22/16 Pct Recovery = 41% Analysis Date = 10/17/16 Pct Recovery = 41% Analysis Date = 10/17/16 Pct Recovery = 41% Analysis Date = 10/13/16 Pct Recovery = 41% Analysis Date = 10/13/16 Pct Recovery = 41% Analysis Date = 10/08/16 Pct Recovery = 41% Analysis Date = 10/08/16 Pct Recovery = 41% Analysis Date = 10/03/16 Pct Recovery = 41% Analysis Date = 10/03/16 Pct Recovery = 41% Analysis Date = 09/28/16 Pct Recovery = 41% Analysis Date = 09/28/16 Pct Recovery = 41% Analysis Date = 09/23/16 Pct Recovery = 41% Analysis Date = 09/23/16 Pct Recovery = 41% Analysis Date = 09/18/16 Pct Recovery = 42% Analysis Date = 09/18/16 Pct Recovery = 42% Analysis Date = 09/13/16 Pct Recovery = 42% Analysis Date = 09/13/16 Pct Recovery = 42% Analysis Date = 09/08/16 Pct Recovery = 42% Analysis Date = 09/08/16 Pct Recovery = 42% Analysis Date = 09/03/16 Pct Recovery = 42% Analysis Date = 09/03/16 Pct Recovery = 42% Analysis Date = 08/29/16 Pct Recovery = 42% Analysis Date = 08/29/16 Pct Recovery = 42% Analysis Date = 08/24/16 Pct Recovery = 42% Analysis Date = 08/24/16 Pct Recovery = 42% Analysis Date = 08/19/16 Pct Recovery = 42% Analysis Date = 08/19/16 Pct Recovery = 42% Analysis Date = 08/14/16 Pct Recovery = 42% Analysis Date = 08/14/16 Pct Recovery = 42% Analysis Date = 08/09/16 Pct Recovery = 42% Analysis Date = 08/09/16 Pct Recovery = 42% Analysis Date = 08/04/16 Pct Recovery = 42% Analysis Date = 08/04/16 Pct Recovery = 42% Analysis Date = 07/30/16 Pct Recovery = 42% Analysis Date = 07/30/16 Pct Recovery = 42% Analysis Date = 07/25/16 Pct Recovery = 43% Analysis Date = 07/25/16 Pct Recovery = 43% Analysis Date = 07/21/16 Pct Recovery = 43% Analysis Date = 07/21/16 Pct Recovery = 43% Analysis Date = 07/16/16 Pct Recovery = 43% Analysis Date = 07/16/16 Pct Recovery = 43% Analysis Date = 07/11/16 Pct Recovery = 43% Analysis Date = 07/11/16 Pct Recovery = 43% Analysis Date = 07/06/16 Pct Recovery = 43% Analysis Date = 07/06/16 Pct Recovery = 43% Analysis Date = 07/01/16 Pct Recovery = 44% Analysis Date = 07/01/16 Pct Recovery = 44% Analysis Date = 06/26/16 Pct Recovery = 44% Analysis Date = 06/26/16 Pct Recovery = 44% Analysis Date = 06/21/16 Pct Recovery = 44% Analysis Date = 06/21/16 Pct Recovery = 44% Analysis Date = 06/16/16 Pct Recovery = 44% Analysis Date = 06/16/16 Pct Recovery = 44% Analysis Date = 06/11/16 Pct Recovery = 44% Analysis Date = 06/11/16 Pct Recovery = 44% Analysis Date = 06/06/16 Pct Recovery = 45% Analysis Date = 06/06/16 Pct Recovery = 45% Analysis Date = 06/01/16 Pct Recovery = 45% Analysis Date = 06/01/16 Pct Recovery = 45% Analysis Date = 05/27/16 Pct Recovery = 45% Analysis Date = 05/27/16 Pct Recovery = 45% Analysis Date = 05/22/16 Pct Recovery = 45% Analysis Date = 05/22/16 Pct Recovery = 45% Analysis Date = 05/17/16 Pct Recovery = 45% Analysis Date = 05/17/16 Pct Recovery = 45% Analysis Date = 05/12/16 Pct Recovery = 46% Analysis Date = 05/12/16 Pct Recovery = 46% Analysis Date = 05/07/16 Pct Recovery = 46% Analysis Date = 05/07/16 Pct Recovery = 46% Analysis Date = 05/02/16 Pct Recovery = 46% Analysis Date = 05/02/16 Pct Recovery = 46% Analysis Date = 04/28/16 Pct Recovery = 46% Analysis Date = 04/28/16 Pct Recovery = 46% Analysis Date = 04/23/16 Pct Recovery = 47% Analysis Date = 04/23/16 Pct Recovery = 47% Analysis Date = 04/18/16 Pct Recovery = 47% Analysis Date = 04/18/16 Pct Recovery = 47% Analysis Date = 04/13/16 Pct Recovery = 47% Analysis Date = 04/13/16 Pct Recovery = 47% Analysis Date = 04/08/16 Pct Recovery = 47% Analysis Date = 04/08/16 Pct Recovery = 47% Analysis Date = 04/03/16 Pct Recovery = 47% Analysis Date = 04/03/16 Pct Recovery = 47% Analysis Date = 03/29/16 Pct Recovery = 48% Analysis Date = 03/29/16 Pct Recovery = 48% Analysis Date = 03/24/16 Pct Recovery = 48% Analysis Date = 03/24/16 Pct Recovery = 48% Analysis Date = 03/19/16 Pct Recovery = 48% Analysis Date = 03/19/16 Pct Recovery = 48% Analysis Date = 03/14/16 Pct Recovery = 48% Analysis Date = 03/14/16 Pct Recovery = 48% Analysis Date = 03/09/16 Pct Recovery = 48% Analysis Date = 03/09/16 Pct Recovery = 48% Analysis Date = 03/04/16 Pct Recovery = 49% Analysis Date = 03/04/16 Pct Recovery = 49% Analysis Date = 02/28/16 Pct Recovery = 49% Analysis Date = 02/28/16 Pct Recovery = 49% Analysis Date = 02/23/16 Pct Recovery = 49% Analysis Date = 02/23/16 Pct Recovery = 49% Analysis Date = 02/18/16 Pct Recovery = 49% Analysis Date = 02/18/16 Pct Recovery = 49% Analysis Date = 02/13/16 Pct Recovery = 50% Analysis Date = 02/13/16 Pct Recovery = 50% Analysis Date = 02/09/16 Pct Recovery = 50% Analysis Date = 02/09/16 Pct Recovery = 50% Analysis Date = 02/04/16 Pct Recovery = 50% Analysis Date = 02/04/16 Pct Recovery = 50% Analysis Date = 01/30/16 Pct Recovery = 50% Analysis Date = 01/30/16 Pct Recovery = 50% Analysis Date = 01/25/16 Pct Recovery = 51% Analysis Date = 01/25/16 Pct Recovery = 51% Analysis Date = 01/20/16 Pct Recovery = 51% Analysis Date = 01/20/16 Pct Recovery = 51% Analysis Date = 01/15/16 Pct Recovery = 51% Analysis Date = 01/15/16 Pct Recovery = 51% Analysis Date = 01/10/16 Pct Recovery = 51% Analysis Date = 01/10/16 Pct Recovery = 51% Analysis Date = 01/05/16 Pct Recovery = 52% Analysis Date = 01/05/16 Pct Recovery = 52% Analysis Date = 12/31/15 Pct Recovery = 52% Analysis Date = 12/31/15 Pct Recovery = 52% Analysis Date = 12/26/15 Pct Recovery = 52% Analysis Date = 12/26/15 Pct Recovery = 52% Analysis Date = 12/21/15 Pct Recovery = 52% Analysis Date = 12/21/15 Pct Recovery = 52% Analysis Date = 12/16/15 Pct Recovery = 53% Analysis Date = 12/16/15 Pct Recovery = 53% Analysis Date = 12/11/15 Pct Recovery = 53% Analysis Date = 12/11/15 Pct Recovery = 53% Analysis Date = 12/06/15 Pct Recovery = 53% Analysis Date = 12/06/15 Pct Recovery = 53% Analysis Date = 12/01/15 Pct Recovery = 54% Analysis Date = 12/01/15 Pct Recovery = 54% Analysis Date = 11/26/15 Pct Recovery = 54% Analysis Date = 11/26/15 Pct Recovery = 54% Analysis Date = 11/21/15 Pct Recovery = 54% Analysis Date = 11/21/15 Pct Recovery = 54% Analysis Date = 11/17/15 Pct Recovery = 54% Analysis Date = 11/17/15 Pct Recovery = 54% Analysis Date = 11/12/15 Pct Recovery = 55% Analysis Date = 11/12/15 Pct Recovery = 55% Analysis Date = 11/07/15 Pct Recovery = 55% Analysis Date = 11/07/15 Pct Recovery = 55% Analysis Date = 11/02/15 Pct Recovery = 55% Analysis Date = 11/02/15 Pct Recovery = 55% Analysis Date = 10/28/15 Pct Recovery = 55% Analysis Date = 10/28/15 Pct Recovery = 55% Analysis Date = 10/23/15 Pct Recovery = 56% Analysis Date = 10/23/15 Pct Recovery = 56% Analysis Date = 10/18/15 Pct Recovery = 56% Analysis Date = 10/18/15 Pct Recovery = 56% Analysis Date = 10/13/15 Pct Recovery = 56% Analysis Date = 10/13/15 Pct Recovery = 56% Analysis Date = 10/08/15 Pct Recovery = 57% Analysis Date = 10/08/15 Pct Recovery = 57% Analysis Date = 10/03/15 Pct Recovery = 57% Analysis Date = 10/03/15 Pct Recovery = 57% Analysis Date = 09/28/15 Pct Recovery = 57% Analysis Date = 09/28/15 Pct Recovery = 57% Analysis Date = 09/23/15 Pct Recovery = 57% Analysis Date = 09/23/15 Pct Recovery = 57% Analysis Date = 09/18/15 Pct Recovery = 58% Analysis Date = 09/18/15 Pct Recovery = 58% Analysis Date = 09/13/15 Pct Recovery = 58% Analysis Date = 09/13/15 Pct Recovery = 58% Analysis Date = 09/08/15 Pct Recovery = 58% Analysis Date = 09/08/15 Pct Recovery = 58% Analysis Date = 09/03/15 Pct Recovery = 58% Analysis Date = 09/03/15 Pct Recovery = 58% Analysis Date = 08/29/15 Pct Recovery = 59% Analysis Date = 08/29/15 Pct Recovery = 59% Analysis Date = 08/25/15 Pct Recovery = 59% Analysis Date = 08/25/15 Pct Recovery = 59% Analysis Date = 08/20/15 Pct Recovery = 59% Analysis Date = 08/20/15 Pct Recovery = 59% Analysis Date = 08/15/15 Pct Recovery = 59% Analysis Date = 08/15/15 Pct Recovery = 59% Analysis Date = 08/10/15 Pct Recovery = 59% Analysis Date = 08/10/15 Pct Recovery = 59% Analysis Date = 08/05/15 Pct Recovery = 59% Analysis Date = 08/05/15 Pct Recovery = 59% Analysis Date = 07/31/15 Pct Recovery = 59% Analysis Date = 07/31/15 Pct Recovery = 59% Analysis Date = 07/26/15 Pct Recovery = 60% Analysis Date = 07/26/15 Pct Recovery = 60% Analysis Date = 07/21/15 Pct Recovery = 60% Analysis Date = 07/21/15 Pct Recovery = 60% Analysis Date = 07/16/15 Pct Recovery = 60% Analysis Date = 07/16/15 Pct Recovery = 60% Analysis Date = 07/11/15 Pct Recovery = 60% Analysis Date = 07/11/15 Pct Recovery = 60% Analysis Date = 07/06/15 Pct Recovery = 60% Analysis Date = 07/06/15 Pct Recovery = 60% Analysis Date = 07/01/15 Pct Recovery = 60% Analysis Date = 07/01/15 Pct Recovery = 60% Analysis Date = 06/26/15 Pct Recovery = 60% Analysis Date = 06/26/15 Pct Recovery = 60% Analysis Date = 06/21/15 Pct Recovery = 60% Analysis Date = 06/21/15 Pct Recovery = 60% Analysis Date = 06/16/15 Pct Recovery = 61% Analysis Date = 06/16/15 Pct Recovery = 61% Analysis Date = 06/11/15 Pct Recovery = 61% Analysis Date = 06/11/15 Pct Recovery = 61% Analysis Date = 06/07/15 Pct Recovery = 61% Analysis Date = 06/07/15 Pct Recovery = 61% Analysis Date = 06/02/15 Pct Recovery = 61% Analysis Date = 06/02/15 Pct Recovery = 61% Analysis Date = 05/28/15 Pct Recovery = 61% Analysis Date = 05/28/15 Pct Recovery = 61% Analysis Date = 05/23/15 Pct Recovery = 61% Analysis Date = 05/23/15 Pct Recovery = 61% Analysis Date = 05/18/15 Pct Recovery = 61% Analysis Date = 05/18/15 Pct Recovery = 61% Analysis Date = 05/13/15 Pct Recovery = 61% Analysis Date = 05/13/15 Pct Recovery = 61% Analysis Date = 05/08/15 Pct Recovery = 62% Analysis Date = 05/08/15 Pct Recovery = 62% Analysis Date = 05/03/15 Pct Recovery = 62% Analysis Date = 05/03/15 Pct Recovery = 62% Analysis Date = 04/28/15 Pct Recovery = 62% Analysis Date = 04/28/15 Pct Recovery = 62% Analysis Date = 04/23/15 Pct Recovery = 62% Analysis Date = 04/23/15 Pct Recovery = 62% Analysis Date = 04/18/15 Pct Recovery = 61% Analysis Date = 04/18/15 Pct Recovery = 61% Analysis Date = 04/13/15 Pct Recovery = 61% Analysis Date = 04/13/15 Pct Recovery = 61% Analysis Date = 04/08/15 Pct Recovery = 61% Analysis Date = 04/08/15 Pct Recovery = 61% Analysis Date = 04/03/15 Pct Recovery = 61% Analysis Date = 04/03/15 Pct Recovery = 61% Analysis Date = 03/29/15 Pct Recovery = 61% Analysis Date = 03/29/15 Pct Recovery = 61% Analysis Date = 03/24/15 Pct Recovery = 61% Analysis Date = 03/24/15 Pct Recovery = 61% Analysis Date = 03/19/15 Pct Recovery = 61% Analysis Date = 03/19/15 Pct Recovery = 61% Analysis Date = 03/15/15 Pct Recovery = 61% Analysis Date = 03/15/15 Pct Recovery = 61% Analysis Date = 03/10/15 Pct Recovery = 61% Analysis Date = 03/10/15 Pct Recovery = 61% Analysis Date = 03/05/15 Pct Recovery = 61% Analysis Date = 03/05/15 Pct Recovery = 61% Analysis Date = 02/28/15 Pct Recovery = 61% Analysis Date = 02/28/15 Pct Recovery = 61% Analysis Date = 02/23/15 Pct Recovery = 61% Analysis Date = 02/23/15 Pct Recovery = 61% Analysis Date = 02/18/15 Pct Recovery = 61% Analysis Date = 02/18/15 Pct Recovery = 61% Analysis Date = 02/13/15 Pct Recovery = 61% Analysis Date = 02/13/15 Pct Recovery = 61% Analysis Date = 02/08/15 Pct Recovery = 60% Analysis Date = 02/08/15 Pct Recovery = 60% Analysis Date = 02/03/15 Pct Recovery = 60% Analysis Date = 02/03/15 Pct Recovery = 60% Analysis Date = 01/29/15 Pct Recovery = 60% Analysis Date = 01/29/15 Pct Recovery = 60% Analysis Date = 01/24/15 Pct Recovery = 60% Analysis Date = 01/24/15 Pct Recovery = 60% Analysis Date = 01/19/15 Pct Recovery = 60% Analysis Date = 01/19/15 Pct Recovery = 60% Analysis Date = 01/14/15 Pct Recovery = 60% Analysis Date = 01/14/15 Pct Recovery = 60% Analysis Date = 01/09/15 Pct Recovery = 60% Analysis Date = 01/09/15 Pct Recovery = 60% Analysis Date = 01/04/15 Pct Recovery = 60% Analysis Date = 01/04/15 Pct Recovery = 60% Analysis Date = 12/30/14 Pct Recovery = 60% Analysis Date = 12/30/14 Pct Recovery = 60% Analysis Date = 12/25/14 Pct Recovery = 59% Analysis Date = 12/25/14 Pct Recovery = 59% Analysis Date = 12/21/14 Pct Recovery = 59% Analysis Date = 12/21/14 Pct Recovery = 59% Analysis Date = 12/16/14 Pct Recovery = 59% Analysis Date = 12/16/14 Pct Recovery = 59% Analysis Date = 12/11/14 Pct Recovery = 59% Analysis Date = 12/11/14 Pct Recovery = 59% Analysis Date = 12/06/14 Pct Recovery = 59% Analysis Date = 12/06/14 Pct Recovery = 59% Analysis Date = 12/01/14 Pct Recovery = 59% Analysis Date = 12/01/14 Pct Recovery = 59% Analysis Date = 11/26/14 Pct Recovery = 59% Analysis Date = 11/26/14 Pct Recovery = 59% Analysis Date = 11/21/14 Pct Recovery = 59% Analysis Date = 11/21/14 Pct Recovery = 59% Analysis Date = 11/16/14 Pct Recovery = 59% Analysis Date = 11/16/14 Pct Recovery = 59% Analysis Date = 11/11/14 Pct Recovery = 59% Analysis Date = 11/11/14 Pct Recovery = 59% Analysis Date = 11/06/14 Pct Recovery = 58% Analysis Date = 11/06/14 Pct Recovery = 58% Analysis Date = 11/01/14 Pct Recovery = 58% Analysis Date = 11/01/14 Pct Recovery = 58% Analysis Date = 10/27/14 Pct Recovery = 58% Analysis Date = 10/27/14 Pct Recovery = 58% Analysis Date = 10/22/14 Pct Recovery = 58% Analysis Date = 10/22/14 Pct Recovery = 58% Analysis Date = 10/17/14 Pct Recovery = 58% Analysis Date = 10/17/14 Pct Recovery = 58% Analysis Date = 10/12/14 Pct Recovery = 58% Analysis Date = 10/12/14 Pct Recovery = 58% Analysis Date = 10/07/14 Pct Recovery = 58% Analysis Date = 10/07/14 Pct Recovery = 58% Analysis Date = 10/03/14 Pct Recovery = 58% Analysis Date = 10/03/14 Pct Recovery = 58% Analysis Date = 09/28/14 Pct Recovery = 58% Analysis Date = 09/28/14 Pct Recovery = 58% Analysis Date = 09/23/14 Pct Recovery = 58% Analysis Date = 09/23/14 Pct Recovery = 58% Analysis Date = 09/18/14 Pct Recovery = 57% Analysis Date = 09/18/14 Pct Recovery = 57% Analysis Date = 09/13/14 Pct Recovery = 57% Analysis Date = 09/13/14 Pct Recovery = 57% Analysis Date = 09/08/14 Pct Recovery = 57% Analysis Date = 09/08/14 Pct Recovery = 57% Analysis Date = 09/03/14 Pct Recovery = 57% Analysis Date = 09/03/14 Pct Recovery = 57% Analysis Date = 08/29/14 Pct Recovery = 57% Analysis Date = 08/29/14 Pct Recovery = 57% Analysis Date = 08/24/14 Pct Recovery = 57% Analysis Date = 08/24/14 Pct Recovery = 57% Analysis Date = 08/19/14 Pct Recovery = 57% Analysis Date = 08/19/14 Pct Recovery = 57% Analysis Date = 08/14/14 Pct Recovery = 57% Analysis Date = 08/14/14 Pct Recovery = 57% Analysis Date = 08/09/14 Pct Recovery = 57% Analysis Date = 08/09/14 Pct Recovery = 57% Analysis Date = 08/04/14 Pct Recovery = 56% Analysis Date = 08/04/14 Pct Recovery = 56% Analysis Date = 07/30/14 Pct Recovery = 56% Analysis Date = 07/30/14 Pct Recovery = 56% Analysis Date = 07/25/14 Pct Recovery = 56% Analysis Date = 07/25/14 Pct Recovery = 56% Analysis Date = 07/20/14 Pct Recovery = 56% Analysis Date = 07/20/14 Pct Recovery = 56% Analysis Date = 07/15/14 Pct Recovery = 56% Analysis Date = 07/15/14 Pct Recovery = 56% Analysis Date = 07/11/14 Pct Recovery = 56% Analysis Date = 07/11/14 Pct Recovery = 56% Analysis Date = 07/06/14 Pct Recovery = 56% Analysis Date = 07/06/14 Pct Recovery = 56% Analysis Date = 07/01/14 Pct Recovery = 56% Analysis Date = 07/01/14 Pct Recovery = 56% Analysis Date = 06/26/14 Pct Recovery = 56% Analysis Date = 06/26/14 Pct Recovery = 56% Analysis Date = 06/21/14 Pct Recovery = 55% Analysis Date = 06/21/14 Pct Recovery = 55% Analysis Date = 06/16/14 Pct Recovery = 55% Analysis Date = 06/16/14 Pct Recovery = 55% Analysis Date = 06/11/14 Pct Recovery = 55% Analysis Date = 06/11/14 Pct Recovery = 55% Analysis Date = 06/06/14 Pct Recovery = 55% Analysis Date = 06/06/14 Pct Recovery = 55% Analysis Date = 06/01/14 Pct Recovery = 55% Analysis Date = 06/01/14 Pct Recovery = 55% Analysis Date = 05/27/14 Pct Recovery = 55% Analysis Date = 05/27/14 Pct Recovery = 55% Analysis Date = 05/22/14 Pct Recovery = 55% Analysis Date = 05/22/14 Pct Recovery = 55% Analysis Date = 05/17/14 Pct Recovery = 55% Analysis Date = 05/17/14 Pct Recovery = 55% Analysis Date = 05/12/14 Pct Recovery = 55% Analysis Date = 05/12/14 Pct Recovery = 55% Analysis Date = 05/07/14 Pct Recovery = 54% Analysis Date = 05/07/14 Pct Recovery = 54% Analysis Date = 05/02/14 Pct Recovery = 54% Analysis Date = 05/02/14 Pct Recovery = 54% Analysis Date = 04/27/14 Pct Recovery = 54% Analysis Date = 04/27/14 Pct Recovery = 54% Analysis Date = 04/23/14 Pct Recovery = 54% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
NICOTINE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 72 52% 26% 47% 22%
Total 72 52% 26% 47% 22%

Sample Statistics
NICOTINE

Characteristic N % % Basis
Plotted 72 94% Spiked
Estimated Values 22 29% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 2 3% Spiked
Spiked 77 .  
False Negatives 3 4% 3 out of 77
Not Spiked 38 .  
False Positives 3 8% 3 out of 38

BQS OBSP Determination:
NIZATIDINE
METHOD: 2440 , TESTIDCODE: 67479LCM56
Open Data Set

Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 38% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 28% Analysis Date = 11/05/15 SpikeMix = ERA 0406-15-08: 80 µl & Abs 052215: 80 µl Pct Recovery = 19% Analysis Date = 11/24/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 16% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 8% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 6% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 16% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 23% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 56% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 58% Analysis Date = 09/24/16 SpikeMix = Crescent EN160610015: 80 µl & Abs 061416: 80 µl Pct Recovery = 57% Analysis Date = 09/24/16 SpikeMix = Abs 061416: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 53% Analysis Date = 12/06/14 SpikeMix = ERA 0318-14-02: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 13% Analysis Date = 10/25/14 SpikeMix = Abs 041614: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 33% Analysis Date = 10/11/14 SpikeMix = ERA 0318-14-02: 60 µl & ERA 0319-14-04: 60 µl Pct Recovery = 37% Analysis Date = 08/28/14 SpikeMix = ERA 0319-14-04: 60 µl & ERA 0319-14-05: 60 µl Pct Recovery = 61% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 10% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 9% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 34% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 39% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 16% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 14% Analysis Date = 04/30/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 84% Analysis Date = 04/10/15 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 48% Analysis Date = 02/10/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 28% Analysis Date = 12/07/14 SpikeMix = ERA 0318-14-02: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 35% Analysis Date = 09/12/14 SpikeMix = Abs 041614: 30 µl & ERA 0319-14-04: 30 µl Pct Recovery = 39% Analysis Date = 08/16/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 72% Analysis Date = 07/13/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 58% Analysis Date = 04/23/14 SpikeMix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.2: 20 µl Pct Recovery = 45% Analysis Date = 10/10/14 SpikeMix = Abs 041714: 30 µl & Abs 041814: 30 µl Pct Recovery = 44% Analysis Date = 06/26/15 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 23% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 80% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 33% Analysis Date = 11/24/15 SpikeMix = ERA 0406-15-09: 20 µl & Abs 050115: 20 µl Pct Recovery = 8% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 11% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 67% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 69% Analysis Date = 12/16/16 Pct Recovery = 44% Analysis Date = 12/11/16 Pct Recovery = 43% Analysis Date = 12/11/16 Pct Recovery = 43% Analysis Date = 12/06/16 Pct Recovery = 43% Analysis Date = 12/06/16 Pct Recovery = 43% Analysis Date = 12/01/16 Pct Recovery = 42% Analysis Date = 12/01/16 Pct Recovery = 42% Analysis Date = 11/26/16 Pct Recovery = 41% Analysis Date = 11/26/16 Pct Recovery = 41% Analysis Date = 11/21/16 Pct Recovery = 41% Analysis Date = 11/21/16 Pct Recovery = 41% Analysis Date = 11/16/16 Pct Recovery = 40% Analysis Date = 11/16/16 Pct Recovery = 40% Analysis Date = 11/12/16 Pct Recovery = 39% Analysis Date = 11/12/16 Pct Recovery = 39% Analysis Date = 11/07/16 Pct Recovery = 38% Analysis Date = 11/07/16 Pct Recovery = 38% Analysis Date = 11/02/16 Pct Recovery = 38% Analysis Date = 11/02/16 Pct Recovery = 38% Analysis Date = 10/28/16 Pct Recovery = 37% Analysis Date = 10/28/16 Pct Recovery = 37% Analysis Date = 10/23/16 Pct Recovery = 37% Analysis Date = 10/23/16 Pct Recovery = 37% Analysis Date = 10/18/16 Pct Recovery = 36% Analysis Date = 10/18/16 Pct Recovery = 36% Analysis Date = 10/14/16 Pct Recovery = 36% Analysis Date = 10/14/16 Pct Recovery = 36% Analysis Date = 10/09/16 Pct Recovery = 35% Analysis Date = 10/09/16 Pct Recovery = 35% Analysis Date = 10/04/16 Pct Recovery = 35% Analysis Date = 10/04/16 Pct Recovery = 35% Analysis Date = 09/29/16 Pct Recovery = 34% Analysis Date = 09/29/16 Pct Recovery = 34% Analysis Date = 09/24/16 Pct Recovery = 34% Analysis Date = 09/24/16 Pct Recovery = 34% Analysis Date = 09/19/16 Pct Recovery = 33% Analysis Date = 09/19/16 Pct Recovery = 33% Analysis Date = 09/15/16 Pct Recovery = 33% Analysis Date = 09/15/16 Pct Recovery = 33% Analysis Date = 09/10/16 Pct Recovery = 32% Analysis Date = 09/10/16 Pct Recovery = 32% Analysis Date = 09/05/16 Pct Recovery = 32% Analysis Date = 09/05/16 Pct Recovery = 32% Analysis Date = 08/31/16 Pct Recovery = 32% Analysis Date = 08/31/16 Pct Recovery = 32% Analysis Date = 08/26/16 Pct Recovery = 32% Analysis Date = 08/26/16 Pct Recovery = 32% Analysis Date = 08/21/16 Pct Recovery = 31% Analysis Date = 08/21/16 Pct Recovery = 31% Analysis Date = 08/17/16 Pct Recovery = 31% Analysis Date = 08/17/16 Pct Recovery = 31% Analysis Date = 08/12/16 Pct Recovery = 31% Analysis Date = 08/12/16 Pct Recovery = 31% Analysis Date = 08/07/16 Pct Recovery = 31% Analysis Date = 08/07/16 Pct Recovery = 31% Analysis Date = 08/02/16 Pct Recovery = 31% Analysis Date = 08/02/16 Pct Recovery = 31% Analysis Date = 07/28/16 Pct Recovery = 31% Analysis Date = 07/28/16 Pct Recovery = 31% Analysis Date = 07/23/16 Pct Recovery = 31% Analysis Date = 07/23/16 Pct Recovery = 31% Analysis Date = 07/18/16 Pct Recovery = 31% Analysis Date = 07/18/16 Pct Recovery = 31% Analysis Date = 07/14/16 Pct Recovery = 31% Analysis Date = 07/14/16 Pct Recovery = 31% Analysis Date = 07/09/16 Pct Recovery = 31% Analysis Date = 07/09/16 Pct Recovery = 31% Analysis Date = 07/04/16 Pct Recovery = 31% Analysis Date = 07/04/16 Pct Recovery = 31% Analysis Date = 06/29/16 Pct Recovery = 31% Analysis Date = 06/29/16 Pct Recovery = 31% Analysis Date = 06/24/16 Pct Recovery = 31% Analysis Date = 06/24/16 Pct Recovery = 31% Analysis Date = 06/19/16 Pct Recovery = 31% Analysis Date = 06/19/16 Pct Recovery = 31% Analysis Date = 06/15/16 Pct Recovery = 31% Analysis Date = 06/15/16 Pct Recovery = 31% Analysis Date = 06/10/16 Pct Recovery = 31% Analysis Date = 06/10/16 Pct Recovery = 31% Analysis Date = 06/05/16 Pct Recovery = 31% Analysis Date = 06/05/16 Pct Recovery = 31% Analysis Date = 05/31/16 Pct Recovery = 31% Analysis Date = 05/31/16 Pct Recovery = 31% Analysis Date = 05/26/16 Pct Recovery = 31% Analysis Date = 05/26/16 Pct Recovery = 31% Analysis Date = 05/21/16 Pct Recovery = 31% Analysis Date = 05/21/16 Pct Recovery = 31% Analysis Date = 05/17/16 Pct Recovery = 31% Analysis Date = 05/17/16 Pct Recovery = 31% Analysis Date = 05/12/16 Pct Recovery = 31% Analysis Date = 05/12/16 Pct Recovery = 31% Analysis Date = 05/07/16 Pct Recovery = 31% Analysis Date = 05/07/16 Pct Recovery = 31% Analysis Date = 05/02/16 Pct Recovery = 31% Analysis Date = 05/02/16 Pct Recovery = 31% Analysis Date = 04/27/16 Pct Recovery = 31% Analysis Date = 04/27/16 Pct Recovery = 31% Analysis Date = 04/22/16 Pct Recovery = 31% Analysis Date = 04/22/16 Pct Recovery = 31% Analysis Date = 04/18/16 Pct Recovery = 31% Analysis Date = 04/18/16 Pct Recovery = 31% Analysis Date = 04/13/16 Pct Recovery = 31% Analysis Date = 04/13/16 Pct Recovery = 31% Analysis Date = 04/08/16 Pct Recovery = 31% Analysis Date = 04/08/16 Pct Recovery = 31% Analysis Date = 04/03/16 Pct Recovery = 31% Analysis Date = 04/03/16 Pct Recovery = 31% Analysis Date = 03/29/16 Pct Recovery = 31% Analysis Date = 03/29/16 Pct Recovery = 31% Analysis Date = 03/24/16 Pct Recovery = 31% Analysis Date = 03/24/16 Pct Recovery = 31% Analysis Date = 03/19/16 Pct Recovery = 32% Analysis Date = 03/19/16 Pct Recovery = 32% Analysis Date = 03/15/16 Pct Recovery = 32% Analysis Date = 03/15/16 Pct Recovery = 32% Analysis Date = 03/10/16 Pct Recovery = 32% Analysis Date = 03/10/16 Pct Recovery = 32% Analysis Date = 03/05/16 Pct Recovery = 32% Analysis Date = 03/05/16 Pct Recovery = 32% Analysis Date = 02/29/16 Pct Recovery = 32% Analysis Date = 02/29/16 Pct Recovery = 32% Analysis Date = 02/24/16 Pct Recovery = 32% Analysis Date = 02/24/16 Pct Recovery = 32% Analysis Date = 02/19/16 Pct Recovery = 32% Analysis Date = 02/19/16 Pct Recovery = 32% Analysis Date = 02/15/16 Pct Recovery = 32% Analysis Date = 02/15/16 Pct Recovery = 32% Analysis Date = 02/10/16 Pct Recovery = 32% Analysis Date = 02/10/16 Pct Recovery = 32% Analysis Date = 02/05/16 Pct Recovery = 32% Analysis Date = 02/05/16 Pct Recovery = 32% Analysis Date = 01/31/16 Pct Recovery = 32% Analysis Date = 01/31/16 Pct Recovery = 32% Analysis Date = 01/26/16 Pct Recovery = 32% Analysis Date = 01/26/16 Pct Recovery = 32% Analysis Date = 01/21/16 Pct Recovery = 32% Analysis Date = 01/21/16 Pct Recovery = 32% Analysis Date = 01/17/16 Pct Recovery = 32% Analysis Date = 01/17/16 Pct Recovery = 32% Analysis Date = 01/12/16 Pct Recovery = 32% Analysis Date = 01/12/16 Pct Recovery = 32% Analysis Date = 01/07/16 Pct Recovery = 32% Analysis Date = 01/07/16 Pct Recovery = 32% Analysis Date = 01/02/16 Pct Recovery = 32% Analysis Date = 01/02/16 Pct Recovery = 32% Analysis Date = 12/28/15 Pct Recovery = 32% Analysis Date = 12/28/15 Pct Recovery = 32% Analysis Date = 12/23/15 Pct Recovery = 32% Analysis Date = 12/23/15 Pct Recovery = 32% Analysis Date = 12/19/15 Pct Recovery = 33% Analysis Date = 12/19/15 Pct Recovery = 33% Analysis Date = 12/14/15 Pct Recovery = 33% Analysis Date = 12/14/15 Pct Recovery = 33% Analysis Date = 12/09/15 Pct Recovery = 33% Analysis Date = 12/09/15 Pct Recovery = 33% Analysis Date = 12/04/15 Pct Recovery = 33% Analysis Date = 12/04/15 Pct Recovery = 33% Analysis Date = 11/29/15 Pct Recovery = 33% Analysis Date = 11/29/15 Pct Recovery = 33% Analysis Date = 11/24/15 Pct Recovery = 33% Analysis Date = 11/24/15 Pct Recovery = 33% Analysis Date = 11/19/15 Pct Recovery = 33% Analysis Date = 11/19/15 Pct Recovery = 33% Analysis Date = 11/15/15 Pct Recovery = 33% Analysis Date = 11/15/15 Pct Recovery = 33% Analysis Date = 11/10/15 Pct Recovery = 33% Analysis Date = 11/10/15 Pct Recovery = 33% Analysis Date = 11/05/15 Pct Recovery = 33% Analysis Date = 11/05/15 Pct Recovery = 33% Analysis Date = 10/31/15 Pct Recovery = 33% Analysis Date = 10/31/15 Pct Recovery = 33% Analysis Date = 10/26/15 Pct Recovery = 33% Analysis Date = 10/26/15 Pct Recovery = 33% Analysis Date = 10/21/15 Pct Recovery = 33% Analysis Date = 10/21/15 Pct Recovery = 33% Analysis Date = 10/17/15 Pct Recovery = 33% Analysis Date = 10/17/15 Pct Recovery = 33% Analysis Date = 10/12/15 Pct Recovery = 33% Analysis Date = 10/12/15 Pct Recovery = 33% Analysis Date = 10/07/15 Pct Recovery = 33% Analysis Date = 10/07/15 Pct Recovery = 33% Analysis Date = 10/02/15 Pct Recovery = 34% Analysis Date = 10/02/15 Pct Recovery = 34% Analysis Date = 09/27/15 Pct Recovery = 34% Analysis Date = 09/27/15 Pct Recovery = 34% Analysis Date = 09/22/15 Pct Recovery = 34% Analysis Date = 09/22/15 Pct Recovery = 34% Analysis Date = 09/18/15 Pct Recovery = 34% Analysis Date = 09/18/15 Pct Recovery = 34% Analysis Date = 09/13/15 Pct Recovery = 34% Analysis Date = 09/13/15 Pct Recovery = 34% Analysis Date = 09/08/15 Pct Recovery = 34% Analysis Date = 09/08/15 Pct Recovery = 34% Analysis Date = 09/03/15 Pct Recovery = 34% Analysis Date = 09/03/15 Pct Recovery = 34% Analysis Date = 08/29/15 Pct Recovery = 34% Analysis Date = 08/29/15 Pct Recovery = 34% Analysis Date = 08/24/15 Pct Recovery = 34% Analysis Date = 08/24/15 Pct Recovery = 34% Analysis Date = 08/20/15 Pct Recovery = 34% Analysis Date = 08/20/15 Pct Recovery = 34% Analysis Date = 08/15/15 Pct Recovery = 34% Analysis Date = 08/15/15 Pct Recovery = 34% Analysis Date = 08/10/15 Pct Recovery = 34% Analysis Date = 08/10/15 Pct Recovery = 34% Analysis Date = 08/05/15 Pct Recovery = 35% Analysis Date = 08/05/15 Pct Recovery = 35% Analysis Date = 07/31/15 Pct Recovery = 35% Analysis Date = 07/31/15 Pct Recovery = 35% Analysis Date = 07/26/15 Pct Recovery = 35% Analysis Date = 07/26/15 Pct Recovery = 35% Analysis Date = 07/21/15 Pct Recovery = 35% Analysis Date = 07/21/15 Pct Recovery = 35% Analysis Date = 07/17/15 Pct Recovery = 35% Analysis Date = 07/17/15 Pct Recovery = 35% Analysis Date = 07/12/15 Pct Recovery = 35% Analysis Date = 07/12/15 Pct Recovery = 35% Analysis Date = 07/07/15 Pct Recovery = 35% Analysis Date = 07/07/15 Pct Recovery = 35% Analysis Date = 07/02/15 Pct Recovery = 35% Analysis Date = 07/02/15 Pct Recovery = 35% Analysis Date = 06/27/15 Pct Recovery = 35% Analysis Date = 06/27/15 Pct Recovery = 35% Analysis Date = 06/22/15 Pct Recovery = 35% Analysis Date = 06/22/15 Pct Recovery = 35% Analysis Date = 06/18/15 Pct Recovery = 35% Analysis Date = 06/18/15 Pct Recovery = 35% Analysis Date = 06/13/15 Pct Recovery = 35% Analysis Date = 06/13/15 Pct Recovery = 35% Analysis Date = 06/08/15 Pct Recovery = 35% Analysis Date = 06/08/15 Pct Recovery = 35% Analysis Date = 06/03/15 Pct Recovery = 36% Analysis Date = 06/03/15 Pct Recovery = 36% Analysis Date = 05/29/15 Pct Recovery = 36% Analysis Date = 05/29/15 Pct Recovery = 36% Analysis Date = 05/24/15 Pct Recovery = 36% Analysis Date = 05/24/15 Pct Recovery = 36% Analysis Date = 05/20/15 Pct Recovery = 36% Analysis Date = 05/20/15 Pct Recovery = 36% Analysis Date = 05/15/15 Pct Recovery = 36% Analysis Date = 05/15/15 Pct Recovery = 36% Analysis Date = 05/10/15 Pct Recovery = 36% Analysis Date = 05/10/15 Pct Recovery = 36% Analysis Date = 05/05/15 Pct Recovery = 36% Analysis Date = 05/05/15 Pct Recovery = 36% Analysis Date = 04/30/15 Pct Recovery = 36% Analysis Date = 04/30/15 Pct Recovery = 36% Analysis Date = 04/25/15 Pct Recovery = 36% Analysis Date = 04/25/15 Pct Recovery = 36% Analysis Date = 04/21/15 Pct Recovery = 37% Analysis Date = 04/21/15 Pct Recovery = 37% Analysis Date = 04/16/15 Pct Recovery = 37% Analysis Date = 04/16/15 Pct Recovery = 37% Analysis Date = 04/11/15 Pct Recovery = 37% Analysis Date = 04/11/15 Pct Recovery = 37% Analysis Date = 04/06/15 Pct Recovery = 37% Analysis Date = 04/06/15 Pct Recovery = 37% Analysis Date = 04/01/15 Pct Recovery = 37% Analysis Date = 04/01/15 Pct Recovery = 37% Analysis Date = 03/27/15 Pct Recovery = 38% Analysis Date = 03/27/15 Pct Recovery = 38% Analysis Date = 03/22/15 Pct Recovery = 38% Analysis Date = 03/22/15 Pct Recovery = 38% Analysis Date = 03/18/15 Pct Recovery = 38% Analysis Date = 03/18/15 Pct Recovery = 38% Analysis Date = 03/13/15 Pct Recovery = 38% Analysis Date = 03/13/15 Pct Recovery = 38% Analysis Date = 03/08/15 Pct Recovery = 38% Analysis Date = 03/08/15 Pct Recovery = 38% Analysis Date = 03/03/15 Pct Recovery = 39% Analysis Date = 03/03/15 Pct Recovery = 39% Analysis Date = 02/26/15 Pct Recovery = 39% Analysis Date = 02/26/15 Pct Recovery = 39% Analysis Date = 02/21/15 Pct Recovery = 39% Analysis Date = 02/21/15 Pct Recovery = 39% Analysis Date = 02/17/15 Pct Recovery = 39% Analysis Date = 02/17/15 Pct Recovery = 39% Analysis Date = 02/12/15 Pct Recovery = 40% Analysis Date = 02/12/15 Pct Recovery = 40% Analysis Date = 02/07/15 Pct Recovery = 40% Analysis Date = 02/07/15 Pct Recovery = 40% Analysis Date = 02/02/15 Pct Recovery = 40% Analysis Date = 02/02/15 Pct Recovery = 40% Analysis Date = 01/28/15 Pct Recovery = 40% Analysis Date = 01/28/15 Pct Recovery = 40% Analysis Date = 01/23/15 Pct Recovery = 40% Analysis Date = 01/23/15 Pct Recovery = 40% Analysis Date = 01/19/15 Pct Recovery = 41% Analysis Date = 01/19/15 Pct Recovery = 41% Analysis Date = 01/14/15 Pct Recovery = 41% Analysis Date = 01/14/15 Pct Recovery = 41% Analysis Date = 01/09/15 Pct Recovery = 41% Analysis Date = 01/09/15 Pct Recovery = 41% Analysis Date = 01/04/15 Pct Recovery = 41% Analysis Date = 01/04/15 Pct Recovery = 41% Analysis Date = 12/30/14 Pct Recovery = 41% Analysis Date = 12/30/14 Pct Recovery = 41% Analysis Date = 12/25/14 Pct Recovery = 42% Analysis Date = 12/25/14 Pct Recovery = 42% Analysis Date = 12/21/14 Pct Recovery = 42% Analysis Date = 12/21/14 Pct Recovery = 42% Analysis Date = 12/16/14 Pct Recovery = 42% Analysis Date = 12/16/14 Pct Recovery = 42% Analysis Date = 12/11/14 Pct Recovery = 42% Analysis Date = 12/11/14 Pct Recovery = 42% Analysis Date = 12/06/14 Pct Recovery = 42% Analysis Date = 12/06/14 Pct Recovery = 42% Analysis Date = 12/01/14 Pct Recovery = 43% Analysis Date = 12/01/14 Pct Recovery = 43% Analysis Date = 11/26/14 Pct Recovery = 43% Analysis Date = 11/26/14 Pct Recovery = 43% Analysis Date = 11/21/14 Pct Recovery = 43% Analysis Date = 11/21/14 Pct Recovery = 43% Analysis Date = 11/17/14 Pct Recovery = 43% Analysis Date = 11/17/14 Pct Recovery = 43% Analysis Date = 11/12/14 Pct Recovery = 44% Analysis Date = 11/12/14 Pct Recovery = 44% Analysis Date = 11/07/14 Pct Recovery = 44% Analysis Date = 11/07/14 Pct Recovery = 44% Analysis Date = 11/02/14 Pct Recovery = 44% Analysis Date = 11/02/14 Pct Recovery = 44% Analysis Date = 10/28/14 Pct Recovery = 44% Analysis Date = 10/28/14 Pct Recovery = 44% Analysis Date = 10/23/14 Pct Recovery = 44% Analysis Date = 10/23/14 Pct Recovery = 44% Analysis Date = 10/19/14 Pct Recovery = 45% Analysis Date = 10/19/14 Pct Recovery = 45% Analysis Date = 10/14/14 Pct Recovery = 45% Analysis Date = 10/14/14 Pct Recovery = 45% Analysis Date = 10/09/14 Pct Recovery = 45% Analysis Date = 10/09/14 Pct Recovery = 45% Analysis Date = 10/04/14 Pct Recovery = 45% Analysis Date = 10/04/14 Pct Recovery = 45% Analysis Date = 09/29/14 Pct Recovery = 45% Analysis Date = 09/29/14 Pct Recovery = 45% Analysis Date = 09/24/14 Pct Recovery = 46% Analysis Date = 09/24/14 Pct Recovery = 46% Analysis Date = 09/20/14 Pct Recovery = 46% Analysis Date = 09/20/14 Pct Recovery = 46% Analysis Date = 09/15/14 Pct Recovery = 46% Analysis Date = 09/15/14 Pct Recovery = 46% Analysis Date = 09/10/14 Pct Recovery = 46% Analysis Date = 09/10/14 Pct Recovery = 46% Analysis Date = 09/05/14 Pct Recovery = 46% Analysis Date = 09/05/14 Pct Recovery = 46% Analysis Date = 08/31/14 Pct Recovery = 47% Analysis Date = 08/31/14 Pct Recovery = 47% Analysis Date = 08/26/14 Pct Recovery = 47% Analysis Date = 08/26/14 Pct Recovery = 47% Analysis Date = 08/22/14 Pct Recovery = 47% Analysis Date = 08/22/14 Pct Recovery = 47% Analysis Date = 08/17/14 Pct Recovery = 47% Analysis Date = 08/17/14 Pct Recovery = 47% Analysis Date = 08/12/14 Pct Recovery = 47% Analysis Date = 08/12/14 Pct Recovery = 47% Analysis Date = 08/07/14 Pct Recovery = 48% Analysis Date = 08/07/14 Pct Recovery = 48% Analysis Date = 08/02/14 Pct Recovery = 48% Analysis Date = 08/02/14 Pct Recovery = 48% Analysis Date = 07/28/14 Pct Recovery = 48% Analysis Date = 07/28/14 Pct Recovery = 48% Analysis Date = 07/23/14 Pct Recovery = 48% Analysis Date = 07/23/14 Pct Recovery = 48% Analysis Date = 07/19/14 Pct Recovery = 49% Analysis Date = 07/19/14 Pct Recovery = 49% Analysis Date = 07/14/14 Pct Recovery = 49% Analysis Date = 07/14/14 Pct Recovery = 49% Analysis Date = 07/09/14 Pct Recovery = 49% Analysis Date = 07/09/14 Pct Recovery = 49% Analysis Date = 07/04/14 Pct Recovery = 49% Analysis Date = 07/04/14 Pct Recovery = 49% Analysis Date = 06/29/14 Pct Recovery = 49% Analysis Date = 06/29/14 Pct Recovery = 49% Analysis Date = 06/24/14 Pct Recovery = 50% Analysis Date = 06/24/14 Pct Recovery = 50% Analysis Date = 06/20/14 Pct Recovery = 50% Analysis Date = 06/20/14 Pct Recovery = 50% Analysis Date = 06/15/14 Pct Recovery = 50% Analysis Date = 06/15/14 Pct Recovery = 50% Analysis Date = 06/10/14 Pct Recovery = 50% Analysis Date = 06/10/14 Pct Recovery = 50% Analysis Date = 06/05/14 Pct Recovery = 50% Analysis Date = 06/05/14 Pct Recovery = 50% Analysis Date = 05/31/14 Pct Recovery = 51% Analysis Date = 05/31/14 Pct Recovery = 51% Analysis Date = 05/26/14 Pct Recovery = 51% Analysis Date = 05/26/14 Pct Recovery = 51% Analysis Date = 05/22/14 Pct Recovery = 51% Analysis Date = 05/22/14 Pct Recovery = 51% Analysis Date = 05/17/14 Pct Recovery = 51% Analysis Date = 05/17/14 Pct Recovery = 51% Analysis Date = 05/12/14 Pct Recovery = 52% Analysis Date = 05/12/14 Pct Recovery = 52% Analysis Date = 05/07/14 Pct Recovery = 52% Analysis Date = 05/07/14 Pct Recovery = 52% Analysis Date = 05/02/14 Pct Recovery = 52% Analysis Date = 05/02/14 Pct Recovery = 52% Analysis Date = 04/27/14 Pct Recovery = 52% Analysis Date = 04/27/14 Pct Recovery = 52% Analysis Date = 04/23/14 Pct Recovery = 52% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
NIZATIDINE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 3 49% 33% 67% 43%
>= Reporting Level 35 35% 21% 34% 27%
Total 38 37% 22% 34% 30%

Sample Statistics
NIZATIDINE

Characteristic N % % Basis
Plotted 38 49% Spiked
Estimated Values 38 49% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 3 4% Spiked
Spiked 77 .  
False Negatives 36 47% 36 out of 77
Not Spiked 38 .  
False Positives 0 0% 0 out of 38

BQS OBSP Determination:
NORDIAZEPAM
METHOD: 2440 , TESTIDCODE: 68252LCM56
Open Data Set

Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 86% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 80% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 90% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 82% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 80 µl & ERA 0406-15-08: 80 µl Pct Recovery = 81% Analysis Date = 11/04/15 SpikeMix = Abs 052215: 80 µl & Abs 050115: 80 µl Pct Recovery = 86% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 71% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 71% Analysis Date = 09/24/16 SpikeMix = Crescent EN160610015: 80 µl & Abs 061416: 80 µl Pct Recovery = 75% Analysis Date = 09/24/16 SpikeMix = Abs 061416: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 76% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 76% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 77% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 92% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 84% Analysis Date = 05/07/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 98% Analysis Date = 03/11/15 SpikeMix = ERA 0318-14-02: 15 µl & Abs 041714: 15 µl Pct Recovery = 94% Analysis Date = 01/16/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 90% Analysis Date = 12/06/14 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 76% Analysis Date = 08/21/14 SpikeMix = ERA 0318-14-02: 60 µl & Abs 041714: 60 µl Pct Recovery = 64% Analysis Date = 07/12/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 80% Analysis Date = 06/11/14 SpikeMix = Abs 041614: 60 µl & Abs 041714: 60 µl Pct Recovery = 85% Analysis Date = 05/21/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 83% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 78% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 70% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 79% Analysis Date = 02/23/16 SpikeMix = Abs 052215: 40 µl & Abs 050115: 40 µl Pct Recovery = 91% Analysis Date = 07/31/15 SpikeMix = ERA 0406-15-09: 40 µl & Abs 050115: 40 µl Pct Recovery = 87% Analysis Date = 07/30/15 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 92% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 82% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 89% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 83% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 79% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 78% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 87% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 81% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 74% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 72% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 74% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 72% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 73% Analysis Date = 11/04/14 SpikeMix = Abs 041714: 8 µl & ERA 0319-14-05: 8 µl Pct Recovery = 75% Analysis Date = 10/10/14 SpikeMix = Abs 041714: 30 µl & Abs 041814: 30 µl Pct Recovery = 75% Analysis Date = 07/20/14 SpikeMix = ERA 0318-14-02: 30 µl & Abs 041714: 30 µl Pct Recovery = 75% Analysis Date = 06/28/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 76% Analysis Date = 05/17/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 86% Analysis Date = 04/23/14 SpikeMix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.2: 20 µl Pct Recovery = 90% Analysis Date = 11/25/15 SpikeMix = Abs 050115: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 79% Analysis Date = 11/24/15 SpikeMix = ERA 0406-15-09: 20 µl & Abs 050115: 20 µl Pct Recovery = 87% Analysis Date = 08/27/15 SpikeMix = Abs 052215: 20 µl & Abs 050115: 20 µl Pct Recovery = 78% Analysis Date = 08/11/15 SpikeMix = Abs 050115: 20 µl & Abs 051315: 20 µl Pct Recovery = 68% Analysis Date = 07/09/15 SpikeMix = Abs 050115: 20 µl & Abs 052215: 20 µl Pct Recovery = 76% Analysis Date = 06/09/15 SpikeMix = Abs 051315: 20 µl & Abs 050115: 20 µl Pct Recovery = 82% Analysis Date = 01/18/17 Pct Recovery = 82% Analysis Date = 01/13/17 Pct Recovery = 82% Analysis Date = 01/13/17 Pct Recovery = 82% Analysis Date = 01/08/17 Pct Recovery = 82% Analysis Date = 01/08/17 Pct Recovery = 82% Analysis Date = 01/03/17 Pct Recovery = 82% Analysis Date = 01/03/17 Pct Recovery = 82% Analysis Date = 12/29/16 Pct Recovery = 82% Analysis Date = 12/29/16 Pct Recovery = 82% Analysis Date = 12/24/16 Pct Recovery = 82% Analysis Date = 12/24/16 Pct Recovery = 82% Analysis Date = 12/19/16 Pct Recovery = 82% Analysis Date = 12/19/16 Pct Recovery = 82% Analysis Date = 12/14/16 Pct Recovery = 81% Analysis Date = 12/14/16 Pct Recovery = 81% Analysis Date = 12/09/16 Pct Recovery = 81% Analysis Date = 12/09/16 Pct Recovery = 81% Analysis Date = 12/04/16 Pct Recovery = 81% Analysis Date = 12/04/16 Pct Recovery = 81% Analysis Date = 11/29/16 Pct Recovery = 81% Analysis Date = 11/29/16 Pct Recovery = 81% Analysis Date = 11/24/16 Pct Recovery = 81% Analysis Date = 11/24/16 Pct Recovery = 81% Analysis Date = 11/19/16 Pct Recovery = 81% Analysis Date = 11/19/16 Pct Recovery = 81% Analysis Date = 11/14/16 Pct Recovery = 81% Analysis Date = 11/14/16 Pct Recovery = 81% Analysis Date = 11/09/16 Pct Recovery = 80% Analysis Date = 11/09/16 Pct Recovery = 80% Analysis Date = 11/04/16 Pct Recovery = 80% Analysis Date = 11/04/16 Pct Recovery = 80% Analysis Date = 10/30/16 Pct Recovery = 80% Analysis Date = 10/30/16 Pct Recovery = 80% Analysis Date = 10/25/16 Pct Recovery = 80% Analysis Date = 10/25/16 Pct Recovery = 80% Analysis Date = 10/20/16 Pct Recovery = 80% Analysis Date = 10/20/16 Pct Recovery = 80% Analysis Date = 10/15/16 Pct Recovery = 80% Analysis Date = 10/15/16 Pct Recovery = 80% Analysis Date = 10/10/16 Pct Recovery = 80% Analysis Date = 10/10/16 Pct Recovery = 80% Analysis Date = 10/05/16 Pct Recovery = 80% Analysis Date = 10/05/16 Pct Recovery = 80% Analysis Date = 09/30/16 Pct Recovery = 79% Analysis Date = 09/30/16 Pct Recovery = 79% Analysis Date = 09/25/16 Pct Recovery = 79% Analysis Date = 09/25/16 Pct Recovery = 79% Analysis Date = 09/20/16 Pct Recovery = 79% Analysis Date = 09/20/16 Pct Recovery = 79% Analysis Date = 09/15/16 Pct Recovery = 79% Analysis Date = 09/15/16 Pct Recovery = 79% Analysis Date = 09/10/16 Pct Recovery = 79% Analysis Date = 09/10/16 Pct Recovery = 79% Analysis Date = 09/05/16 Pct Recovery = 79% Analysis Date = 09/05/16 Pct Recovery = 79% Analysis Date = 08/31/16 Pct Recovery = 79% Analysis Date = 08/31/16 Pct Recovery = 79% Analysis Date = 08/26/16 Pct Recovery = 79% Analysis Date = 08/26/16 Pct Recovery = 79% Analysis Date = 08/21/16 Pct Recovery = 79% Analysis Date = 08/21/16 Pct Recovery = 79% Analysis Date = 08/16/16 Pct Recovery = 79% Analysis Date = 08/16/16 Pct Recovery = 79% Analysis Date = 08/11/16 Pct Recovery = 79% Analysis Date = 08/11/16 Pct Recovery = 79% Analysis Date = 08/06/16 Pct Recovery = 79% Analysis Date = 08/06/16 Pct Recovery = 79% Analysis Date = 08/01/16 Pct Recovery = 79% Analysis Date = 08/01/16 Pct Recovery = 79% Analysis Date = 07/27/16 Pct Recovery = 78% Analysis Date = 07/27/16 Pct Recovery = 78% Analysis Date = 07/22/16 Pct Recovery = 78% Analysis Date = 07/22/16 Pct Recovery = 78% Analysis Date = 07/17/16 Pct Recovery = 78% Analysis Date = 07/17/16 Pct Recovery = 78% Analysis Date = 07/12/16 Pct Recovery = 79% Analysis Date = 07/12/16 Pct Recovery = 79% Analysis Date = 07/07/16 Pct Recovery = 79% Analysis Date = 07/07/16 Pct Recovery = 79% Analysis Date = 07/02/16 Pct Recovery = 79% Analysis Date = 07/02/16 Pct Recovery = 79% Analysis Date = 06/27/16 Pct Recovery = 79% Analysis Date = 06/27/16 Pct Recovery = 79% Analysis Date = 06/22/16 Pct Recovery = 79% Analysis Date = 06/22/16 Pct Recovery = 79% Analysis Date = 06/17/16 Pct Recovery = 79% Analysis Date = 06/17/16 Pct Recovery = 79% Analysis Date = 06/12/16 Pct Recovery = 79% Analysis Date = 06/12/16 Pct Recovery = 79% Analysis Date = 06/07/16 Pct Recovery = 79% Analysis Date = 06/07/16 Pct Recovery = 79% Analysis Date = 06/02/16 Pct Recovery = 79% Analysis Date = 06/02/16 Pct Recovery = 79% Analysis Date = 05/28/16 Pct Recovery = 79% Analysis Date = 05/28/16 Pct Recovery = 79% Analysis Date = 05/23/16 Pct Recovery = 79% Analysis Date = 05/23/16 Pct Recovery = 79% Analysis Date = 05/18/16 Pct Recovery = 79% Analysis Date = 05/18/16 Pct Recovery = 79% Analysis Date = 05/13/16 Pct Recovery = 80% Analysis Date = 05/13/16 Pct Recovery = 80% Analysis Date = 05/08/16 Pct Recovery = 80% Analysis Date = 05/08/16 Pct Recovery = 80% Analysis Date = 05/03/16 Pct Recovery = 80% Analysis Date = 05/03/16 Pct Recovery = 80% Analysis Date = 04/28/16 Pct Recovery = 80% Analysis Date = 04/28/16 Pct Recovery = 80% Analysis Date = 04/23/16 Pct Recovery = 80% Analysis Date = 04/23/16 Pct Recovery = 80% Analysis Date = 04/18/16 Pct Recovery = 80% Analysis Date = 04/18/16 Pct Recovery = 80% Analysis Date = 04/13/16 Pct Recovery = 80% Analysis Date = 04/13/16 Pct Recovery = 80% Analysis Date = 04/08/16 Pct Recovery = 80% Analysis Date = 04/08/16 Pct Recovery = 80% Analysis Date = 04/03/16 Pct Recovery = 80% Analysis Date = 04/03/16 Pct Recovery = 80% Analysis Date = 03/29/16 Pct Recovery = 80% Analysis Date = 03/29/16 Pct Recovery = 80% Analysis Date = 03/24/16 Pct Recovery = 80% Analysis Date = 03/24/16 Pct Recovery = 80% Analysis Date = 03/19/16 Pct Recovery = 80% Analysis Date = 03/19/16 Pct Recovery = 80% Analysis Date = 03/14/16 Pct Recovery = 81% Analysis Date = 03/14/16 Pct Recovery = 81% Analysis Date = 03/09/16 Pct Recovery = 81% Analysis Date = 03/09/16 Pct Recovery = 81% Analysis Date = 03/04/16 Pct Recovery = 81% Analysis Date = 03/04/16 Pct Recovery = 81% Analysis Date = 02/28/16 Pct Recovery = 81% Analysis Date = 02/28/16 Pct Recovery = 81% Analysis Date = 02/23/16 Pct Recovery = 81% Analysis Date = 02/23/16 Pct Recovery = 81% Analysis Date = 02/18/16 Pct Recovery = 81% Analysis Date = 02/18/16 Pct Recovery = 81% Analysis Date = 02/13/16 Pct Recovery = 81% Analysis Date = 02/13/16 Pct Recovery = 81% Analysis Date = 02/08/16 Pct Recovery = 81% Analysis Date = 02/08/16 Pct Recovery = 81% Analysis Date = 02/03/16 Pct Recovery = 81% Analysis Date = 02/03/16 Pct Recovery = 81% Analysis Date = 01/29/16 Pct Recovery = 81% Analysis Date = 01/29/16 Pct Recovery = 81% Analysis Date = 01/24/16 Pct Recovery = 81% Analysis Date = 01/24/16 Pct Recovery = 81% Analysis Date = 01/19/16 Pct Recovery = 81% Analysis Date = 01/19/16 Pct Recovery = 81% Analysis Date = 01/14/16 Pct Recovery = 81% Analysis Date = 01/14/16 Pct Recovery = 81% Analysis Date = 01/09/16 Pct Recovery = 82% Analysis Date = 01/09/16 Pct Recovery = 82% Analysis Date = 01/04/16 Pct Recovery = 82% Analysis Date = 01/04/16 Pct Recovery = 82% Analysis Date = 12/30/15 Pct Recovery = 82% Analysis Date = 12/30/15 Pct Recovery = 82% Analysis Date = 12/25/15 Pct Recovery = 82% Analysis Date = 12/25/15 Pct Recovery = 82% Analysis Date = 12/20/15 Pct Recovery = 82% Analysis Date = 12/20/15 Pct Recovery = 82% Analysis Date = 12/15/15 Pct Recovery = 82% Analysis Date = 12/15/15 Pct Recovery = 82% Analysis Date = 12/10/15 Pct Recovery = 82% Analysis Date = 12/10/15 Pct Recovery = 82% Analysis Date = 12/05/15 Pct Recovery = 82% Analysis Date = 12/05/15 Pct Recovery = 82% Analysis Date = 11/30/15 Pct Recovery = 82% Analysis Date = 11/30/15 Pct Recovery = 82% Analysis Date = 11/25/15 Pct Recovery = 82% Analysis Date = 11/25/15 Pct Recovery = 82% Analysis Date = 11/20/15 Pct Recovery = 82% Analysis Date = 11/20/15 Pct Recovery = 82% Analysis Date = 11/15/15 Pct Recovery = 82% Analysis Date = 11/15/15 Pct Recovery = 82% Analysis Date = 11/10/15 Pct Recovery = 82% Analysis Date = 11/10/15 Pct Recovery = 82% Analysis Date = 11/05/15 Pct Recovery = 82% Analysis Date = 11/05/15 Pct Recovery = 82% Analysis Date = 10/31/15 Pct Recovery = 83% Analysis Date = 10/31/15 Pct Recovery = 83% Analysis Date = 10/26/15 Pct Recovery = 83% Analysis Date = 10/26/15 Pct Recovery = 83% Analysis Date = 10/21/15 Pct Recovery = 83% Analysis Date = 10/21/15 Pct Recovery = 83% Analysis Date = 10/16/15 Pct Recovery = 83% Analysis Date = 10/16/15 Pct Recovery = 83% Analysis Date = 10/11/15 Pct Recovery = 83% Analysis Date = 10/11/15 Pct Recovery = 83% Analysis Date = 10/06/15 Pct Recovery = 83% Analysis Date = 10/06/15 Pct Recovery = 83% Analysis Date = 10/01/15 Pct Recovery = 83% Analysis Date = 10/01/15 Pct Recovery = 83% Analysis Date = 09/26/15 Pct Recovery = 83% Analysis Date = 09/26/15 Pct Recovery = 83% Analysis Date = 09/21/15 Pct Recovery = 83% Analysis Date = 09/21/15 Pct Recovery = 83% Analysis Date = 09/16/15 Pct Recovery = 83% Analysis Date = 09/16/15 Pct Recovery = 83% Analysis Date = 09/11/15 Pct Recovery = 83% Analysis Date = 09/11/15 Pct Recovery = 83% Analysis Date = 09/05/15 Pct Recovery = 83% Analysis Date = 09/05/15 Pct Recovery = 83% Analysis Date = 08/31/15 Pct Recovery = 83% Analysis Date = 08/31/15 Pct Recovery = 83% Analysis Date = 08/26/15 Pct Recovery = 84% Analysis Date = 08/26/15 Pct Recovery = 84% Analysis Date = 08/21/15 Pct Recovery = 83% Analysis Date = 08/21/15 Pct Recovery = 83% Analysis Date = 08/16/15 Pct Recovery = 83% Analysis Date = 08/16/15 Pct Recovery = 83% Analysis Date = 08/11/15 Pct Recovery = 83% Analysis Date = 08/11/15 Pct Recovery = 83% Analysis Date = 08/06/15 Pct Recovery = 83% Analysis Date = 08/06/15 Pct Recovery = 83% Analysis Date = 08/01/15 Pct Recovery = 83% Analysis Date = 08/01/15 Pct Recovery = 83% Analysis Date = 07/27/15 Pct Recovery = 83% Analysis Date = 07/27/15 Pct Recovery = 83% Analysis Date = 07/22/15 Pct Recovery = 83% Analysis Date = 07/22/15 Pct Recovery = 83% Analysis Date = 07/17/15 Pct Recovery = 83% Analysis Date = 07/17/15 Pct Recovery = 83% Analysis Date = 07/12/15 Pct Recovery = 83% Analysis Date = 07/12/15 Pct Recovery = 83% Analysis Date = 07/07/15 Pct Recovery = 83% Analysis Date = 07/07/15 Pct Recovery = 83% Analysis Date = 07/02/15 Pct Recovery = 83% Analysis Date = 07/02/15 Pct Recovery = 83% Analysis Date = 06/27/15 Pct Recovery = 83% Analysis Date = 06/27/15 Pct Recovery = 83% Analysis Date = 06/22/15 Pct Recovery = 83% Analysis Date = 06/22/15 Pct Recovery = 83% Analysis Date = 06/17/15 Pct Recovery = 83% Analysis Date = 06/17/15 Pct Recovery = 83% Analysis Date = 06/12/15 Pct Recovery = 83% Analysis Date = 06/12/15 Pct Recovery = 83% Analysis Date = 06/07/15 Pct Recovery = 83% Analysis Date = 06/07/15 Pct Recovery = 83% Analysis Date = 06/02/15 Pct Recovery = 83% Analysis Date = 06/02/15 Pct Recovery = 83% Analysis Date = 05/28/15 Pct Recovery = 83% Analysis Date = 05/28/15 Pct Recovery = 83% Analysis Date = 05/23/15 Pct Recovery = 83% Analysis Date = 05/23/15 Pct Recovery = 83% Analysis Date = 05/18/15 Pct Recovery = 82% Analysis Date = 05/18/15 Pct Recovery = 82% Analysis Date = 05/13/15 Pct Recovery = 82% Analysis Date = 05/13/15 Pct Recovery = 82% Analysis Date = 05/08/15 Pct Recovery = 82% Analysis Date = 05/08/15 Pct Recovery = 82% Analysis Date = 05/03/15 Pct Recovery = 82% Analysis Date = 05/03/15 Pct Recovery = 82% Analysis Date = 04/28/15 Pct Recovery = 82% Analysis Date = 04/28/15 Pct Recovery = 82% Analysis Date = 04/23/15 Pct Recovery = 82% Analysis Date = 04/23/15 Pct Recovery = 82% Analysis Date = 04/18/15 Pct Recovery = 82% Analysis Date = 04/18/15 Pct Recovery = 82% Analysis Date = 04/13/15 Pct Recovery = 82% Analysis Date = 04/13/15 Pct Recovery = 82% Analysis Date = 04/08/15 Pct Recovery = 82% Analysis Date = 04/08/15 Pct Recovery = 82% Analysis Date = 04/03/15 Pct Recovery = 82% Analysis Date = 04/03/15 Pct Recovery = 82% Analysis Date = 03/29/15 Pct Recovery = 82% Analysis Date = 03/29/15 Pct Recovery = 82% Analysis Date = 03/24/15 Pct Recovery = 82% Analysis Date = 03/24/15 Pct Recovery = 82% Analysis Date = 03/19/15 Pct Recovery = 82% Analysis Date = 03/19/15 Pct Recovery = 82% Analysis Date = 03/14/15 Pct Recovery = 82% Analysis Date = 03/14/15 Pct Recovery = 82% Analysis Date = 03/09/15 Pct Recovery = 82% Analysis Date = 03/09/15 Pct Recovery = 82% Analysis Date = 03/04/15 Pct Recovery = 82% Analysis Date = 03/04/15 Pct Recovery = 82% Analysis Date = 02/27/15 Pct Recovery = 82% Analysis Date = 02/27/15 Pct Recovery = 82% Analysis Date = 02/22/15 Pct Recovery = 82% Analysis Date = 02/22/15 Pct Recovery = 82% Analysis Date = 02/17/15 Pct Recovery = 82% Analysis Date = 02/17/15 Pct Recovery = 82% Analysis Date = 02/12/15 Pct Recovery = 82% Analysis Date = 02/12/15 Pct Recovery = 82% Analysis Date = 02/07/15 Pct Recovery = 82% Analysis Date = 02/07/15 Pct Recovery = 82% Analysis Date = 02/02/15 Pct Recovery = 82% Analysis Date = 02/02/15 Pct Recovery = 82% Analysis Date = 01/28/15 Pct Recovery = 82% Analysis Date = 01/28/15 Pct Recovery = 82% Analysis Date = 01/23/15 Pct Recovery = 81% Analysis Date = 01/23/15 Pct Recovery = 81% Analysis Date = 01/18/15 Pct Recovery = 81% Analysis Date = 01/18/15 Pct Recovery = 81% Analysis Date = 01/13/15 Pct Recovery = 81% Analysis Date = 01/13/15 Pct Recovery = 81% Analysis Date = 01/08/15 Pct Recovery = 81% Analysis Date = 01/08/15 Pct Recovery = 81% Analysis Date = 01/03/15 Pct Recovery = 81% Analysis Date = 01/03/15 Pct Recovery = 81% Analysis Date = 12/29/14 Pct Recovery = 81% Analysis Date = 12/29/14 Pct Recovery = 81% Analysis Date = 12/24/14 Pct Recovery = 81% Analysis Date = 12/24/14 Pct Recovery = 81% Analysis Date = 12/19/14 Pct Recovery = 81% Analysis Date = 12/19/14 Pct Recovery = 81% Analysis Date = 12/14/14 Pct Recovery = 81% Analysis Date = 12/14/14 Pct Recovery = 81% Analysis Date = 12/09/14 Pct Recovery = 81% Analysis Date = 12/09/14 Pct Recovery = 81% Analysis Date = 12/04/14 Pct Recovery = 81% Analysis Date = 12/04/14 Pct Recovery = 81% Analysis Date = 11/29/14 Pct Recovery = 81% Analysis Date = 11/29/14 Pct Recovery = 81% Analysis Date = 11/24/14 Pct Recovery = 81% Analysis Date = 11/24/14 Pct Recovery = 81% Analysis Date = 11/19/14 Pct Recovery = 81% Analysis Date = 11/19/14 Pct Recovery = 81% Analysis Date = 11/14/14 Pct Recovery = 81% Analysis Date = 11/14/14 Pct Recovery = 81% Analysis Date = 11/09/14 Pct Recovery = 81% Analysis Date = 11/09/14 Pct Recovery = 81% Analysis Date = 11/04/14 Pct Recovery = 81% Analysis Date = 11/04/14 Pct Recovery = 81% Analysis Date = 10/30/14 Pct Recovery = 81% Analysis Date = 10/30/14 Pct Recovery = 81% Analysis Date = 10/25/14 Pct Recovery = 81% Analysis Date = 10/25/14 Pct Recovery = 81% Analysis Date = 10/20/14 Pct Recovery = 81% Analysis Date = 10/20/14 Pct Recovery = 81% Analysis Date = 10/15/14 Pct Recovery = 81% Analysis Date = 10/15/14 Pct Recovery = 81% Analysis Date = 10/10/14 Pct Recovery = 81% Analysis Date = 10/10/14 Pct Recovery = 81% Analysis Date = 10/05/14 Pct Recovery = 81% Analysis Date = 10/05/14 Pct Recovery = 81% Analysis Date = 09/30/14 Pct Recovery = 81% Analysis Date = 09/30/14 Pct Recovery = 81% Analysis Date = 09/25/14 Pct Recovery = 81% Analysis Date = 09/25/14 Pct Recovery = 81% Analysis Date = 09/20/14 Pct Recovery = 81% Analysis Date = 09/20/14 Pct Recovery = 81% Analysis Date = 09/15/14 Pct Recovery = 81% Analysis Date = 09/15/14 Pct Recovery = 81% Analysis Date = 09/10/14 Pct Recovery = 81% Analysis Date = 09/10/14 Pct Recovery = 81% Analysis Date = 09/05/14 Pct Recovery = 81% Analysis Date = 09/05/14 Pct Recovery = 81% Analysis Date = 08/31/14 Pct Recovery = 81% Analysis Date = 08/31/14 Pct Recovery = 81% Analysis Date = 08/26/14 Pct Recovery = 81% Analysis Date = 08/26/14 Pct Recovery = 81% Analysis Date = 08/21/14 Pct Recovery = 81% Analysis Date = 08/21/14 Pct Recovery = 81% Analysis Date = 08/16/14 Pct Recovery = 81% Analysis Date = 08/16/14 Pct Recovery = 81% Analysis Date = 08/11/14 Pct Recovery = 81% Analysis Date = 08/11/14 Pct Recovery = 81% Analysis Date = 08/06/14 Pct Recovery = 81% Analysis Date = 08/06/14 Pct Recovery = 81% Analysis Date = 08/01/14 Pct Recovery = 81% Analysis Date = 08/01/14 Pct Recovery = 81% Analysis Date = 07/27/14 Pct Recovery = 81% Analysis Date = 07/27/14 Pct Recovery = 81% Analysis Date = 07/22/14 Pct Recovery = 81% Analysis Date = 07/22/14 Pct Recovery = 81% Analysis Date = 07/17/14 Pct Recovery = 81% Analysis Date = 07/17/14 Pct Recovery = 81% Analysis Date = 07/12/14 Pct Recovery = 81% Analysis Date = 07/12/14 Pct Recovery = 81% Analysis Date = 07/07/14 Pct Recovery = 80% Analysis Date = 07/07/14 Pct Recovery = 80% Analysis Date = 07/02/14 Pct Recovery = 80% Analysis Date = 07/02/14 Pct Recovery = 80% Analysis Date = 06/27/14 Pct Recovery = 80% Analysis Date = 06/27/14 Pct Recovery = 80% Analysis Date = 06/22/14 Pct Recovery = 80% Analysis Date = 06/22/14 Pct Recovery = 80% Analysis Date = 06/17/14 Pct Recovery = 80% Analysis Date = 06/17/14 Pct Recovery = 80% Analysis Date = 06/12/14 Pct Recovery = 80% Analysis Date = 06/12/14 Pct Recovery = 80% Analysis Date = 06/07/14 Pct Recovery = 80% Analysis Date = 06/07/14 Pct Recovery = 80% Analysis Date = 06/02/14 Pct Recovery = 80% Analysis Date = 06/02/14 Pct Recovery = 80% Analysis Date = 05/28/14 Pct Recovery = 80% Analysis Date = 05/28/14 Pct Recovery = 80% Analysis Date = 05/23/14 Pct Recovery = 80% Analysis Date = 05/23/14 Pct Recovery = 80% Analysis Date = 05/18/14 Pct Recovery = 80% Analysis Date = 05/18/14 Pct Recovery = 80% Analysis Date = 05/13/14 Pct Recovery = 80% Analysis Date = 05/13/14 Pct Recovery = 80% Analysis Date = 05/08/14 Pct Recovery = 80% Analysis Date = 05/08/14 Pct Recovery = 80% Analysis Date = 05/03/14 Pct Recovery = 80% Analysis Date = 05/03/14 Pct Recovery = 80% Analysis Date = 04/28/14 Pct Recovery = 80% Analysis Date = 04/28/14 Pct Recovery = 80% Analysis Date = 04/23/14 Pct Recovery = 80% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
NORDIAZEPAM

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 52 81% 7% 80% 8%
Total 52 81% 7% 80% 8%

Sample Statistics
NORDIAZEPAM

Characteristic N % % Basis
Plotted 52 100% Spiked
Estimated Values 11 21% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 52 .  
False Negatives 0 0% 0 out of 52
Not Spiked 63 .  
False Positives 0 0% 0 out of 63

BQS OBSP Determination:
NORETHINDRONE
METHOD: 2440 , TESTIDCODE: 67434LCM56
Open Data Set

Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 78% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 82% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 94% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 89% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 80 µl & ERA 0406-15-08: 80 µl Pct Recovery = 84% Analysis Date = 11/05/15 SpikeMix = ERA 0406-15-08: 80 µl & Abs 052215: 80 µl Pct Recovery = 73% Analysis Date = 11/24/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 75% Analysis Date = 10/03/15 SpikeMix = ERA 0406-15-07A: 80 µl & Abs 051315: 80 µl Pct Recovery = 132% Analysis Date = 10/01/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 129% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 58% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 67% Analysis Date = 09/24/16 SpikeMix = Crescent EN160610015: 80 µl & Abs 061416: 80 µl Pct Recovery = 71% Analysis Date = 09/24/16 SpikeMix = Abs 061416: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 69% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 57% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 71% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 86% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 84% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 49% Analysis Date = 12/07/14 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 75% Analysis Date = 10/25/14 SpikeMix = Abs 041614: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 68% Analysis Date = 06/22/14 SpikeMix = Abs 041814: 60 µl & Abs 041614: 60 µl Pct Recovery = 104% Analysis Date = 06/11/14 SpikeMix = Abs 041614: 60 µl & Abs 041714: 60 µl Pct Recovery = 75% Analysis Date = 04/29/15 SpikeMix = ERA 0319-14-05: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 76% Analysis Date = 03/11/15 SpikeMix = ERA 0318-14-02: 15 µl & Abs 041714: 15 µl Pct Recovery = 62% Analysis Date = 02/06/15 SpikeMix = Abs 041814: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 77% Analysis Date = 12/06/14 SpikeMix = ERA 0318-14-02: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 72% Analysis Date = 10/11/14 SpikeMix = ERA 0318-14-02: 60 µl & ERA 0319-14-04: 60 µl Pct Recovery = 61% Analysis Date = 08/21/14 SpikeMix = ERA 0318-14-02: 60 µl & Abs 041714: 60 µl Pct Recovery = 67% Analysis Date = 07/26/14 SpikeMix = ERA 0319-14-05: 60 µl & ERA 0318-14-02: 60 µl Pct Recovery = 88% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 77% Analysis Date = 11/04/15 SpikeMix = ERA 0406-15-07A: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 68% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-08: 40 µl & ERA 0406-15-09: 40 µl Pct Recovery = 105% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 85% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 68% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-07A: 40 µl & Abs 051315: 40 µl Pct Recovery = 74% Analysis Date = 07/30/15 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 52% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 82% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 84% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 73% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 77% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 64% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 71% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 69% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 65% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 62% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 65% Analysis Date = 04/30/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 38% Analysis Date = 02/10/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 68% Analysis Date = 10/24/14 SpikeMix = ERA 0319-14-05: 8 µl & Abs 041614: 8 µl Pct Recovery = 52% Analysis Date = 12/07/14 SpikeMix = ERA 0318-14-02: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 77% Analysis Date = 11/04/14 SpikeMix = Abs 041814: 8 µl & ERA 0318-14-02: 8 µl Pct Recovery = 80% Analysis Date = 09/12/14 SpikeMix = Abs 041614: 30 µl & ERA 0319-14-04: 30 µl Pct Recovery = 49% Analysis Date = 07/13/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 60% Analysis Date = 06/28/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 74% Analysis Date = 05/30/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 75% Analysis Date = 05/17/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 68% Analysis Date = 10/10/14 SpikeMix = Abs 041814: 30 µl & ERA 0318-14-02: 30 µl Pct Recovery = 50% Analysis Date = 08/30/14 SpikeMix = ERA 0318-14-02: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 69% Analysis Date = 07/20/14 SpikeMix = ERA 0318-14-02: 30 µl & Abs 041714: 30 µl Pct Recovery = 64% Analysis Date = 04/27/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 106% Analysis Date = 11/25/15 SpikeMix = Abs 050115: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 88% Analysis Date = 09/15/15 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 58% Analysis Date = 09/10/15 SpikeMix = ERA 0406-15-08: 20 µl & Abs 052215: 20 µl Pct Recovery = 76% Analysis Date = 02/23/16 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 95% Analysis Date = 08/13/15 SpikeMix = Abs 050115: 20 µl & Abs 051315: 20 µl Pct Recovery = 35% Analysis Date = 06/29/15 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 61% Analysis Date = 06/09/15 SpikeMix = Abs 051315: 20 µl & Abs 050115: 20 µl Pct Recovery = 97% Analysis Date = 01/18/17 Pct Recovery = 73% Analysis Date = 01/14/17 Pct Recovery = 73% Analysis Date = 01/14/17 Pct Recovery = 73% Analysis Date = 01/09/17 Pct Recovery = 73% Analysis Date = 01/09/17 Pct Recovery = 73% Analysis Date = 01/04/17 Pct Recovery = 73% Analysis Date = 01/04/17 Pct Recovery = 73% Analysis Date = 12/30/16 Pct Recovery = 74% Analysis Date = 12/30/16 Pct Recovery = 74% Analysis Date = 12/25/16 Pct Recovery = 74% Analysis Date = 12/25/16 Pct Recovery = 74% Analysis Date = 12/20/16 Pct Recovery = 74% Analysis Date = 12/20/16 Pct Recovery = 74% Analysis Date = 12/15/16 Pct Recovery = 74% Analysis Date = 12/15/16 Pct Recovery = 74% Analysis Date = 12/10/16 Pct Recovery = 74% Analysis Date = 12/10/16 Pct Recovery = 74% Analysis Date = 12/05/16 Pct Recovery = 74% Analysis Date = 12/05/16 Pct Recovery = 74% Analysis Date = 12/01/16 Pct Recovery = 74% Analysis Date = 12/01/16 Pct Recovery = 74% Analysis Date = 11/26/16 Pct Recovery = 74% Analysis Date = 11/26/16 Pct Recovery = 74% Analysis Date = 11/21/16 Pct Recovery = 74% Analysis Date = 11/21/16 Pct Recovery = 74% Analysis Date = 11/16/16 Pct Recovery = 74% Analysis Date = 11/16/16 Pct Recovery = 74% Analysis Date = 11/11/16 Pct Recovery = 74% Analysis Date = 11/11/16 Pct Recovery = 74% Analysis Date = 11/06/16 Pct Recovery = 74% Analysis Date = 11/06/16 Pct Recovery = 74% Analysis Date = 11/01/16 Pct Recovery = 74% Analysis Date = 11/01/16 Pct Recovery = 74% Analysis Date = 10/27/16 Pct Recovery = 75% Analysis Date = 10/27/16 Pct Recovery = 75% Analysis Date = 10/22/16 Pct Recovery = 75% Analysis Date = 10/22/16 Pct Recovery = 75% Analysis Date = 10/18/16 Pct Recovery = 75% Analysis Date = 10/18/16 Pct Recovery = 75% Analysis Date = 10/13/16 Pct Recovery = 75% Analysis Date = 10/13/16 Pct Recovery = 75% Analysis Date = 10/08/16 Pct Recovery = 75% Analysis Date = 10/08/16 Pct Recovery = 75% Analysis Date = 10/03/16 Pct Recovery = 75% Analysis Date = 10/03/16 Pct Recovery = 75% Analysis Date = 09/28/16 Pct Recovery = 75% Analysis Date = 09/28/16 Pct Recovery = 75% Analysis Date = 09/23/16 Pct Recovery = 75% Analysis Date = 09/23/16 Pct Recovery = 75% Analysis Date = 09/18/16 Pct Recovery = 75% Analysis Date = 09/18/16 Pct Recovery = 75% Analysis Date = 09/13/16 Pct Recovery = 75% Analysis Date = 09/13/16 Pct Recovery = 75% Analysis Date = 09/08/16 Pct Recovery = 76% Analysis Date = 09/08/16 Pct Recovery = 76% Analysis Date = 09/04/16 Pct Recovery = 76% Analysis Date = 09/04/16 Pct Recovery = 76% Analysis Date = 08/30/16 Pct Recovery = 76% Analysis Date = 08/30/16 Pct Recovery = 76% Analysis Date = 08/25/16 Pct Recovery = 76% Analysis Date = 08/25/16 Pct Recovery = 76% Analysis Date = 08/20/16 Pct Recovery = 76% Analysis Date = 08/20/16 Pct Recovery = 76% Analysis Date = 08/15/16 Pct Recovery = 76% Analysis Date = 08/15/16 Pct Recovery = 76% Analysis Date = 08/10/16 Pct Recovery = 76% Analysis Date = 08/10/16 Pct Recovery = 76% Analysis Date = 08/05/16 Pct Recovery = 77% Analysis Date = 08/05/16 Pct Recovery = 77% Analysis Date = 07/31/16 Pct Recovery = 77% Analysis Date = 07/31/16 Pct Recovery = 77% Analysis Date = 07/26/16 Pct Recovery = 77% Analysis Date = 07/26/16 Pct Recovery = 77% Analysis Date = 07/22/16 Pct Recovery = 77% Analysis Date = 07/22/16 Pct Recovery = 77% Analysis Date = 07/17/16 Pct Recovery = 77% Analysis Date = 07/17/16 Pct Recovery = 77% Analysis Date = 07/12/16 Pct Recovery = 77% Analysis Date = 07/12/16 Pct Recovery = 77% Analysis Date = 07/07/16 Pct Recovery = 77% Analysis Date = 07/07/16 Pct Recovery = 77% Analysis Date = 07/02/16 Pct Recovery = 78% Analysis Date = 07/02/16 Pct Recovery = 78% Analysis Date = 06/27/16 Pct Recovery = 78% Analysis Date = 06/27/16 Pct Recovery = 78% Analysis Date = 06/22/16 Pct Recovery = 78% Analysis Date = 06/22/16 Pct Recovery = 78% Analysis Date = 06/17/16 Pct Recovery = 78% Analysis Date = 06/17/16 Pct Recovery = 78% Analysis Date = 06/12/16 Pct Recovery = 78% Analysis Date = 06/12/16 Pct Recovery = 78% Analysis Date = 06/08/16 Pct Recovery = 78% Analysis Date = 06/08/16 Pct Recovery = 78% Analysis Date = 06/03/16 Pct Recovery = 78% Analysis Date = 06/03/16 Pct Recovery = 78% Analysis Date = 05/29/16 Pct Recovery = 79% Analysis Date = 05/29/16 Pct Recovery = 79% Analysis Date = 05/24/16 Pct Recovery = 79% Analysis Date = 05/24/16 Pct Recovery = 79% Analysis Date = 05/19/16 Pct Recovery = 79% Analysis Date = 05/19/16 Pct Recovery = 79% Analysis Date = 05/14/16 Pct Recovery = 79% Analysis Date = 05/14/16 Pct Recovery = 79% Analysis Date = 05/09/16 Pct Recovery = 79% Analysis Date = 05/09/16 Pct Recovery = 79% Analysis Date = 05/04/16 Pct Recovery = 79% Analysis Date = 05/04/16 Pct Recovery = 79% Analysis Date = 04/29/16 Pct Recovery = 79% Analysis Date = 04/29/16 Pct Recovery = 79% Analysis Date = 04/25/16 Pct Recovery = 80% Analysis Date = 04/25/16 Pct Recovery = 80% Analysis Date = 04/20/16 Pct Recovery = 80% Analysis Date = 04/20/16 Pct Recovery = 80% Analysis Date = 04/15/16 Pct Recovery = 80% Analysis Date = 04/15/16 Pct Recovery = 80% Analysis Date = 04/10/16 Pct Recovery = 80% Analysis Date = 04/10/16 Pct Recovery = 80% Analysis Date = 04/05/16 Pct Recovery = 80% Analysis Date = 04/05/16 Pct Recovery = 80% Analysis Date = 03/31/16 Pct Recovery = 80% Analysis Date = 03/31/16 Pct Recovery = 80% Analysis Date = 03/26/16 Pct Recovery = 80% Analysis Date = 03/26/16 Pct Recovery = 80% Analysis Date = 03/21/16 Pct Recovery = 80% Analysis Date = 03/21/16 Pct Recovery = 80% Analysis Date = 03/16/16 Pct Recovery = 80% Analysis Date = 03/16/16 Pct Recovery = 80% Analysis Date = 03/12/16 Pct Recovery = 80% Analysis Date = 03/12/16 Pct Recovery = 80% Analysis Date = 03/07/16 Pct Recovery = 80% Analysis Date = 03/07/16 Pct Recovery = 80% Analysis Date = 03/02/16 Pct Recovery = 80% Analysis Date = 03/02/16 Pct Recovery = 80% Analysis Date = 02/26/16 Pct Recovery = 80% Analysis Date = 02/26/16 Pct Recovery = 80% Analysis Date = 02/21/16 Pct Recovery = 80% Analysis Date = 02/21/16 Pct Recovery = 80% Analysis Date = 02/16/16 Pct Recovery = 81% Analysis Date = 02/16/16 Pct Recovery = 81% Analysis Date = 02/11/16 Pct Recovery = 81% Analysis Date = 02/11/16 Pct Recovery = 81% Analysis Date = 02/06/16 Pct Recovery = 81% Analysis Date = 02/06/16 Pct Recovery = 81% Analysis Date = 02/01/16 Pct Recovery = 81% Analysis Date = 02/01/16 Pct Recovery = 81% Analysis Date = 01/28/16 Pct Recovery = 81% Analysis Date = 01/28/16 Pct Recovery = 81% Analysis Date = 01/23/16 Pct Recovery = 81% Analysis Date = 01/23/16 Pct Recovery = 81% Analysis Date = 01/18/16 Pct Recovery = 81% Analysis Date = 01/18/16 Pct Recovery = 81% Analysis Date = 01/13/16 Pct Recovery = 81% Analysis Date = 01/13/16 Pct Recovery = 81% Analysis Date = 01/08/16 Pct Recovery = 81% Analysis Date = 01/08/16 Pct Recovery = 81% Analysis Date = 01/03/16 Pct Recovery = 81% Analysis Date = 01/03/16 Pct Recovery = 81% Analysis Date = 12/29/15 Pct Recovery = 81% Analysis Date = 12/29/15 Pct Recovery = 81% Analysis Date = 12/24/15 Pct Recovery = 81% Analysis Date = 12/24/15 Pct Recovery = 81% Analysis Date = 12/19/15 Pct Recovery = 81% Analysis Date = 12/19/15 Pct Recovery = 81% Analysis Date = 12/15/15 Pct Recovery = 81% Analysis Date = 12/15/15 Pct Recovery = 81% Analysis Date = 12/10/15 Pct Recovery = 81% Analysis Date = 12/10/15 Pct Recovery = 81% Analysis Date = 12/05/15 Pct Recovery = 81% Analysis Date = 12/05/15 Pct Recovery = 81% Analysis Date = 11/30/15 Pct Recovery = 81% Analysis Date = 11/30/15 Pct Recovery = 81% Analysis Date = 11/25/15 Pct Recovery = 81% Analysis Date = 11/25/15 Pct Recovery = 81% Analysis Date = 11/20/15 Pct Recovery = 80% Analysis Date = 11/20/15 Pct Recovery = 80% Analysis Date = 11/15/15 Pct Recovery = 80% Analysis Date = 11/15/15 Pct Recovery = 80% Analysis Date = 11/10/15 Pct Recovery = 80% Analysis Date = 11/10/15 Pct Recovery = 80% Analysis Date = 11/05/15 Pct Recovery = 80% Analysis Date = 11/05/15 Pct Recovery = 80% Analysis Date = 11/01/15 Pct Recovery = 80% Analysis Date = 11/01/15 Pct Recovery = 80% Analysis Date = 10/27/15 Pct Recovery = 79% Analysis Date = 10/27/15 Pct Recovery = 79% Analysis Date = 10/22/15 Pct Recovery = 79% Analysis Date = 10/22/15 Pct Recovery = 79% Analysis Date = 10/17/15 Pct Recovery = 79% Analysis Date = 10/17/15 Pct Recovery = 79% Analysis Date = 10/12/15 Pct Recovery = 79% Analysis Date = 10/12/15 Pct Recovery = 79% Analysis Date = 10/07/15 Pct Recovery = 79% Analysis Date = 10/07/15 Pct Recovery = 79% Analysis Date = 10/02/15 Pct Recovery = 78% Analysis Date = 10/02/15 Pct Recovery = 78% Analysis Date = 09/27/15 Pct Recovery = 78% Analysis Date = 09/27/15 Pct Recovery = 78% Analysis Date = 09/22/15 Pct Recovery = 78% Analysis Date = 09/22/15 Pct Recovery = 78% Analysis Date = 09/17/15 Pct Recovery = 78% Analysis Date = 09/17/15 Pct Recovery = 78% Analysis Date = 09/13/15 Pct Recovery = 77% Analysis Date = 09/13/15 Pct Recovery = 77% Analysis Date = 09/08/15 Pct Recovery = 77% Analysis Date = 09/08/15 Pct Recovery = 77% Analysis Date = 09/03/15 Pct Recovery = 77% Analysis Date = 09/03/15 Pct Recovery = 77% Analysis Date = 08/29/15 Pct Recovery = 77% Analysis Date = 08/29/15 Pct Recovery = 77% Analysis Date = 08/24/15 Pct Recovery = 76% Analysis Date = 08/24/15 Pct Recovery = 76% Analysis Date = 08/19/15 Pct Recovery = 76% Analysis Date = 08/19/15 Pct Recovery = 76% Analysis Date = 08/14/15 Pct Recovery = 76% Analysis Date = 08/14/15 Pct Recovery = 76% Analysis Date = 08/09/15 Pct Recovery = 76% Analysis Date = 08/09/15 Pct Recovery = 76% Analysis Date = 08/04/15 Pct Recovery = 76% Analysis Date = 08/04/15 Pct Recovery = 76% Analysis Date = 07/31/15 Pct Recovery = 75% Analysis Date = 07/31/15 Pct Recovery = 75% Analysis Date = 07/26/15 Pct Recovery = 75% Analysis Date = 07/26/15 Pct Recovery = 75% Analysis Date = 07/21/15 Pct Recovery = 75% Analysis Date = 07/21/15 Pct Recovery = 75% Analysis Date = 07/16/15 Pct Recovery = 75% Analysis Date = 07/16/15 Pct Recovery = 75% Analysis Date = 07/11/15 Pct Recovery = 74% Analysis Date = 07/11/15 Pct Recovery = 74% Analysis Date = 07/06/15 Pct Recovery = 74% Analysis Date = 07/06/15 Pct Recovery = 74% Analysis Date = 07/01/15 Pct Recovery = 74% Analysis Date = 07/01/15 Pct Recovery = 74% Analysis Date = 06/26/15 Pct Recovery = 74% Analysis Date = 06/26/15 Pct Recovery = 74% Analysis Date = 06/21/15 Pct Recovery = 74% Analysis Date = 06/21/15 Pct Recovery = 74% Analysis Date = 06/17/15 Pct Recovery = 73% Analysis Date = 06/17/15 Pct Recovery = 73% Analysis Date = 06/12/15 Pct Recovery = 73% Analysis Date = 06/12/15 Pct Recovery = 73% Analysis Date = 06/07/15 Pct Recovery = 73% Analysis Date = 06/07/15 Pct Recovery = 73% Analysis Date = 06/02/15 Pct Recovery = 73% Analysis Date = 06/02/15 Pct Recovery = 73% Analysis Date = 05/28/15 Pct Recovery = 73% Analysis Date = 05/28/15 Pct Recovery = 73% Analysis Date = 05/23/15 Pct Recovery = 72% Analysis Date = 05/23/15 Pct Recovery = 72% Analysis Date = 05/18/15 Pct Recovery = 72% Analysis Date = 05/18/15 Pct Recovery = 72% Analysis Date = 05/13/15 Pct Recovery = 72% Analysis Date = 05/13/15 Pct Recovery = 72% Analysis Date = 05/08/15 Pct Recovery = 72% Analysis Date = 05/08/15 Pct Recovery = 72% Analysis Date = 05/04/15 Pct Recovery = 72% Analysis Date = 05/04/15 Pct Recovery = 72% Analysis Date = 04/29/15 Pct Recovery = 71% Analysis Date = 04/29/15 Pct Recovery = 71% Analysis Date = 04/24/15 Pct Recovery = 71% Analysis Date = 04/24/15 Pct Recovery = 71% Analysis Date = 04/19/15 Pct Recovery = 71% Analysis Date = 04/19/15 Pct Recovery = 71% Analysis Date = 04/14/15 Pct Recovery = 71% Analysis Date = 04/14/15 Pct Recovery = 71% Analysis Date = 04/09/15 Pct Recovery = 71% Analysis Date = 04/09/15 Pct Recovery = 71% Analysis Date = 04/04/15 Pct Recovery = 71% Analysis Date = 04/04/15 Pct Recovery = 71% Analysis Date = 03/30/15 Pct Recovery = 70% Analysis Date = 03/30/15 Pct Recovery = 70% Analysis Date = 03/25/15 Pct Recovery = 70% Analysis Date = 03/25/15 Pct Recovery = 70% Analysis Date = 03/21/15 Pct Recovery = 70% Analysis Date = 03/21/15 Pct Recovery = 70% Analysis Date = 03/16/15 Pct Recovery = 70% Analysis Date = 03/16/15 Pct Recovery = 70% Analysis Date = 03/11/15 Pct Recovery = 70% Analysis Date = 03/11/15 Pct Recovery = 70% Analysis Date = 03/06/15 Pct Recovery = 70% Analysis Date = 03/06/15 Pct Recovery = 70% Analysis Date = 03/01/15 Pct Recovery = 70% Analysis Date = 03/01/15 Pct Recovery = 70% Analysis Date = 02/24/15 Pct Recovery = 70% Analysis Date = 02/24/15 Pct Recovery = 70% Analysis Date = 02/19/15 Pct Recovery = 70% Analysis Date = 02/19/15 Pct Recovery = 70% Analysis Date = 02/14/15 Pct Recovery = 70% Analysis Date = 02/14/15 Pct Recovery = 70% Analysis Date = 02/09/15 Pct Recovery = 69% Analysis Date = 02/09/15 Pct Recovery = 69% Analysis Date = 02/05/15 Pct Recovery = 69% Analysis Date = 02/05/15 Pct Recovery = 69% Analysis Date = 01/31/15 Pct Recovery = 69% Analysis Date = 01/31/15 Pct Recovery = 69% Analysis Date = 01/26/15 Pct Recovery = 69% Analysis Date = 01/26/15 Pct Recovery = 69% Analysis Date = 01/21/15 Pct Recovery = 69% Analysis Date = 01/21/15 Pct Recovery = 69% Analysis Date = 01/16/15 Pct Recovery = 69% Analysis Date = 01/16/15 Pct Recovery = 69% Analysis Date = 01/11/15 Pct Recovery = 69% Analysis Date = 01/11/15 Pct Recovery = 69% Analysis Date = 01/06/15 Pct Recovery = 69% Analysis Date = 01/06/15 Pct Recovery = 69% Analysis Date = 01/01/15 Pct Recovery = 69% Analysis Date = 01/01/15 Pct Recovery = 69% Analysis Date = 12/27/14 Pct Recovery = 69% Analysis Date = 12/27/14 Pct Recovery = 69% Analysis Date = 12/23/14 Pct Recovery = 69% Analysis Date = 12/23/14 Pct Recovery = 69% Analysis Date = 12/18/14 Pct Recovery = 69% Analysis Date = 12/18/14 Pct Recovery = 69% Analysis Date = 12/13/14 Pct Recovery = 69% Analysis Date = 12/13/14 Pct Recovery = 69% Analysis Date = 12/08/14 Pct Recovery = 69% Analysis Date = 12/08/14 Pct Recovery = 69% Analysis Date = 12/03/14 Pct Recovery = 69% Analysis Date = 12/03/14 Pct Recovery = 69% Analysis Date = 11/28/14 Pct Recovery = 69% Analysis Date = 11/28/14 Pct Recovery = 69% Analysis Date = 11/23/14 Pct Recovery = 69% Analysis Date = 11/23/14 Pct Recovery = 69% Analysis Date = 11/18/14 Pct Recovery = 69% Analysis Date = 11/18/14 Pct Recovery = 69% Analysis Date = 11/13/14 Pct Recovery = 69% Analysis Date = 11/13/14 Pct Recovery = 69% Analysis Date = 11/09/14 Pct Recovery = 69% Analysis Date = 11/09/14 Pct Recovery = 69% Analysis Date = 11/04/14 Pct Recovery = 69% Analysis Date = 11/04/14 Pct Recovery = 69% Analysis Date = 10/30/14 Pct Recovery = 69% Analysis Date = 10/30/14 Pct Recovery = 69% Analysis Date = 10/25/14 Pct Recovery = 69% Analysis Date = 10/25/14 Pct Recovery = 69% Analysis Date = 10/20/14 Pct Recovery = 69% Analysis Date = 10/20/14 Pct Recovery = 69% Analysis Date = 10/15/14 Pct Recovery = 69% Analysis Date = 10/15/14 Pct Recovery = 69% Analysis Date = 10/10/14 Pct Recovery = 69% Analysis Date = 10/10/14 Pct Recovery = 69% Analysis Date = 10/05/14 Pct Recovery = 69% Analysis Date = 10/05/14 Pct Recovery = 69% Analysis Date = 09/30/14 Pct Recovery = 69% Analysis Date = 09/30/14 Pct Recovery = 69% Analysis Date = 09/26/14 Pct Recovery = 69% Analysis Date = 09/26/14 Pct Recovery = 69% Analysis Date = 09/21/14 Pct Recovery = 69% Analysis Date = 09/21/14 Pct Recovery = 69% Analysis Date = 09/16/14 Pct Recovery = 69% Analysis Date = 09/16/14 Pct Recovery = 69% Analysis Date = 09/11/14 Pct Recovery = 69% Analysis Date = 09/11/14 Pct Recovery = 69% Analysis Date = 09/06/14 Pct Recovery = 69% Analysis Date = 09/06/14 Pct Recovery = 69% Analysis Date = 09/01/14 Pct Recovery = 69% Analysis Date = 09/01/14 Pct Recovery = 69% Analysis Date = 08/27/14 Pct Recovery = 69% Analysis Date = 08/27/14 Pct Recovery = 69% Analysis Date = 08/22/14 Pct Recovery = 69% Analysis Date = 08/22/14 Pct Recovery = 69% Analysis Date = 08/17/14 Pct Recovery = 69% Analysis Date = 08/17/14 Pct Recovery = 69% Analysis Date = 08/13/14 Pct Recovery = 69% Analysis Date = 08/13/14 Pct Recovery = 69% Analysis Date = 08/08/14 Pct Recovery = 70% Analysis Date = 08/08/14 Pct Recovery = 70% Analysis Date = 08/03/14 Pct Recovery = 70% Analysis Date = 08/03/14 Pct Recovery = 70% Analysis Date = 07/29/14 Pct Recovery = 70% Analysis Date = 07/29/14 Pct Recovery = 70% Analysis Date = 07/24/14 Pct Recovery = 70% Analysis Date = 07/24/14 Pct Recovery = 70% Analysis Date = 07/19/14 Pct Recovery = 70% Analysis Date = 07/19/14 Pct Recovery = 70% Analysis Date = 07/14/14 Pct Recovery = 70% Analysis Date = 07/14/14 Pct Recovery = 70% Analysis Date = 07/09/14 Pct Recovery = 70% Analysis Date = 07/09/14 Pct Recovery = 70% Analysis Date = 07/04/14 Pct Recovery = 70% Analysis Date = 07/04/14 Pct Recovery = 70% Analysis Date = 06/30/14 Pct Recovery = 70% Analysis Date = 06/30/14 Pct Recovery = 70% Analysis Date = 06/25/14 Pct Recovery = 70% Analysis Date = 06/25/14 Pct Recovery = 70% Analysis Date = 06/20/14 Pct Recovery = 70% Analysis Date = 06/20/14 Pct Recovery = 70% Analysis Date = 06/15/14 Pct Recovery = 70% Analysis Date = 06/15/14 Pct Recovery = 70% Analysis Date = 06/10/14 Pct Recovery = 70% Analysis Date = 06/10/14 Pct Recovery = 70% Analysis Date = 06/05/14 Pct Recovery = 70% Analysis Date = 06/05/14 Pct Recovery = 70% Analysis Date = 05/31/14 Pct Recovery = 70% Analysis Date = 05/31/14 Pct Recovery = 70% Analysis Date = 05/26/14 Pct Recovery = 70% Analysis Date = 05/26/14 Pct Recovery = 70% Analysis Date = 05/21/14 Pct Recovery = 70% Analysis Date = 05/21/14 Pct Recovery = 70% Analysis Date = 05/17/14 Pct Recovery = 70% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
NORETHINDRONE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 67 74% 17% 73% 13%
Total 67 74% 17% 73% 13%

Sample Statistics
NORETHINDRONE

Characteristic N % % Basis
Plotted 67 89% Spiked
Estimated Values 8 11% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 6 8% Spiked
Spiked 75 .  
False Negatives 2 3% 2 out of 75
Not Spiked 40 .  
False Positives 0 0% 0 out of 40

BQS OBSP Determination:
NORFLUOXETINE
METHOD: 2440 , TESTIDCODE: 67451LCM56
Open Data Set

Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 73% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 87% Analysis Date = 01/17/16 SpikeMix = ERA 0406-15-09: 80 µl & ERA 0406-15-07A: 80 µl Pct Recovery = 71% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 80 µl & Abs 051315: 80 µl Pct Recovery = 69% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 80 µl & ERA 0406-15-08: 80 µl Pct Recovery = 60% Analysis Date = 11/04/15 SpikeMix = Abs 052215: 80 µl & Abs 050115: 80 µl Pct Recovery = 57% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 62% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 66% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 50% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 57% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-04: 15 µl & Abs 041814: 15 µl Pct Recovery = 71% Analysis Date = 12/06/14 SpikeMix = ERA 0318-14-02: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 70% Analysis Date = 10/25/14 SpikeMix = Abs 041614: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 91% Analysis Date = 10/11/14 SpikeMix = ERA 0318-14-02: 60 µl & ERA 0319-14-04: 60 µl Pct Recovery = 91% Analysis Date = 08/28/14 SpikeMix = ERA 0319-14-04: 60 µl & ERA 0319-14-05: 60 µl Pct Recovery = 70% Analysis Date = 05/07/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 63% Analysis Date = 03/11/15 SpikeMix = ERA 0318-14-02: 15 µl & Abs 041714: 15 µl Pct Recovery = 64% Analysis Date = 01/16/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 49% Analysis Date = 12/06/14 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 43% Analysis Date = 08/21/14 SpikeMix = ERA 0318-14-02: 60 µl & Abs 041714: 60 µl Pct Recovery = 41% Analysis Date = 07/12/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 52% Analysis Date = 06/11/14 SpikeMix = Abs 041614: 60 µl & Abs 041714: 60 µl Pct Recovery = 59% Analysis Date = 05/21/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 61% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-07A: 40 µl & Abs 051315: 40 µl Pct Recovery = 47% Analysis Date = 11/04/15 SpikeMix = ERA 0406-15-07A: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 58% Analysis Date = 09/10/15 SpikeMix = Abs 052215: 40 µl & ERA 0406-15-07A: 40 µl Pct Recovery = 63% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 60% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 53% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 50% Analysis Date = 02/23/16 SpikeMix = Abs 052215: 40 µl & Abs 050115: 40 µl Pct Recovery = 65% Analysis Date = 07/31/15 SpikeMix = ERA 0406-15-09: 40 µl & Abs 050115: 40 µl Pct Recovery = 72% Analysis Date = 07/30/15 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 71% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 59% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 73% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 56% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 58% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 36% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 38% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 53% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 62% Analysis Date = 04/30/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 82% Analysis Date = 04/10/15 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 77% Analysis Date = 02/10/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 57% Analysis Date = 12/07/14 SpikeMix = ERA 0318-14-02: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 86% Analysis Date = 10/11/14 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 87% Analysis Date = 11/04/14 SpikeMix = Abs 041714: 8 µl & ERA 0319-14-05: 8 µl Pct Recovery = 37% Analysis Date = 09/12/14 SpikeMix = Abs 041614: 30 µl & ERA 0319-14-04: 30 µl Pct Recovery = 79% Analysis Date = 08/16/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 57% Analysis Date = 07/13/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 43% Analysis Date = 10/10/14 SpikeMix = Abs 041714: 30 µl & Abs 041814: 30 µl Pct Recovery = 70% Analysis Date = 07/20/14 SpikeMix = ERA 0318-14-02: 30 µl & Abs 041714: 30 µl Pct Recovery = 47% Analysis Date = 06/28/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 53% Analysis Date = 05/17/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 52% Analysis Date = 04/23/14 SpikeMix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.2: 20 µl Pct Recovery = 85% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 56% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 48% Analysis Date = 04/27/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 75% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 58% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 47% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 46% Analysis Date = 11/24/15 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 45% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-09: 20 µl Pct Recovery = 68% Analysis Date = 09/15/15 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 56% Analysis Date = 11/25/15 SpikeMix = Abs 050115: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 41% Analysis Date = 11/24/15 SpikeMix = ERA 0406-15-09: 20 µl & Abs 050115: 20 µl Pct Recovery = 56% Analysis Date = 08/27/15 SpikeMix = Abs 052215: 20 µl & Abs 050115: 20 µl Pct Recovery = 46% Analysis Date = 08/11/15 SpikeMix = Abs 050115: 20 µl & Abs 051315: 20 µl Pct Recovery = 39% Analysis Date = 07/09/15 SpikeMix = Abs 050115: 20 µl & Abs 052215: 20 µl Pct Recovery = 53% Analysis Date = 06/09/15 SpikeMix = Abs 051315: 20 µl & Abs 050115: 20 µl Pct Recovery = 60% Analysis Date = 01/18/17 Pct Recovery = 66% Analysis Date = 01/13/17 Pct Recovery = 66% Analysis Date = 01/13/17 Pct Recovery = 66% Analysis Date = 01/08/17 Pct Recovery = 66% Analysis Date = 01/08/17 Pct Recovery = 66% Analysis Date = 01/03/17 Pct Recovery = 66% Analysis Date = 01/03/17 Pct Recovery = 66% Analysis Date = 12/29/16 Pct Recovery = 65% Analysis Date = 12/29/16 Pct Recovery = 65% Analysis Date = 12/24/16 Pct Recovery = 65% Analysis Date = 12/24/16 Pct Recovery = 65% Analysis Date = 12/19/16 Pct Recovery = 65% Analysis Date = 12/19/16 Pct Recovery = 65% Analysis Date = 12/14/16 Pct Recovery = 65% Analysis Date = 12/14/16 Pct Recovery = 65% Analysis Date = 12/09/16 Pct Recovery = 65% Analysis Date = 12/09/16 Pct Recovery = 65% Analysis Date = 12/04/16 Pct Recovery = 64% Analysis Date = 12/04/16 Pct Recovery = 64% Analysis Date = 11/29/16 Pct Recovery = 64% Analysis Date = 11/29/16 Pct Recovery = 64% Analysis Date = 11/24/16 Pct Recovery = 64% Analysis Date = 11/24/16 Pct Recovery = 64% Analysis Date = 11/19/16 Pct Recovery = 64% Analysis Date = 11/19/16 Pct Recovery = 64% Analysis Date = 11/14/16 Pct Recovery = 63% Analysis Date = 11/14/16 Pct Recovery = 63% Analysis Date = 11/09/16 Pct Recovery = 63% Analysis Date = 11/09/16 Pct Recovery = 63% Analysis Date = 11/04/16 Pct Recovery = 63% Analysis Date = 11/04/16 Pct Recovery = 63% Analysis Date = 10/30/16 Pct Recovery = 63% Analysis Date = 10/30/16 Pct Recovery = 63% Analysis Date = 10/25/16 Pct Recovery = 63% Analysis Date = 10/25/16 Pct Recovery = 63% Analysis Date = 10/20/16 Pct Recovery = 62% Analysis Date = 10/20/16 Pct Recovery = 62% Analysis Date = 10/15/16 Pct Recovery = 62% Analysis Date = 10/15/16 Pct Recovery = 62% Analysis Date = 10/10/16 Pct Recovery = 62% Analysis Date = 10/10/16 Pct Recovery = 62% Analysis Date = 10/05/16 Pct Recovery = 62% Analysis Date = 10/05/16 Pct Recovery = 62% Analysis Date = 09/30/16 Pct Recovery = 61% Analysis Date = 09/30/16 Pct Recovery = 61% Analysis Date = 09/25/16 Pct Recovery = 61% Analysis Date = 09/25/16 Pct Recovery = 61% Analysis Date = 09/20/16 Pct Recovery = 61% Analysis Date = 09/20/16 Pct Recovery = 61% Analysis Date = 09/15/16 Pct Recovery = 61% Analysis Date = 09/15/16 Pct Recovery = 61% Analysis Date = 09/10/16 Pct Recovery = 61% Analysis Date = 09/10/16 Pct Recovery = 61% Analysis Date = 09/05/16 Pct Recovery = 60% Analysis Date = 09/05/16 Pct Recovery = 60% Analysis Date = 08/31/16 Pct Recovery = 60% Analysis Date = 08/31/16 Pct Recovery = 60% Analysis Date = 08/26/16 Pct Recovery = 60% Analysis Date = 08/26/16 Pct Recovery = 60% Analysis Date = 08/21/16 Pct Recovery = 60% Analysis Date = 08/21/16 Pct Recovery = 60% Analysis Date = 08/16/16 Pct Recovery = 59% Analysis Date = 08/16/16 Pct Recovery = 59% Analysis Date = 08/11/16 Pct Recovery = 59% Analysis Date = 08/11/16 Pct Recovery = 59% Analysis Date = 08/06/16 Pct Recovery = 59% Analysis Date = 08/06/16 Pct Recovery = 59% Analysis Date = 08/01/16 Pct Recovery = 59% Analysis Date = 08/01/16 Pct Recovery = 59% Analysis Date = 07/27/16 Pct Recovery = 59% Analysis Date = 07/27/16 Pct Recovery = 59% Analysis Date = 07/22/16 Pct Recovery = 58% Analysis Date = 07/22/16 Pct Recovery = 58% Analysis Date = 07/17/16 Pct Recovery = 58% Analysis Date = 07/17/16 Pct Recovery = 58% Analysis Date = 07/12/16 Pct Recovery = 58% Analysis Date = 07/12/16 Pct Recovery = 58% Analysis Date = 07/07/16 Pct Recovery = 58% Analysis Date = 07/07/16 Pct Recovery = 58% Analysis Date = 07/02/16 Pct Recovery = 58% Analysis Date = 07/02/16 Pct Recovery = 58% Analysis Date = 06/27/16 Pct Recovery = 58% Analysis Date = 06/27/16 Pct Recovery = 58% Analysis Date = 06/22/16 Pct Recovery = 57% Analysis Date = 06/22/16 Pct Recovery = 57% Analysis Date = 06/17/16 Pct Recovery = 57% Analysis Date = 06/17/16 Pct Recovery = 57% Analysis Date = 06/12/16 Pct Recovery = 57% Analysis Date = 06/12/16 Pct Recovery = 57% Analysis Date = 06/07/16 Pct Recovery = 57% Analysis Date = 06/07/16 Pct Recovery = 57% Analysis Date = 06/02/16 Pct Recovery = 57% Analysis Date = 06/02/16 Pct Recovery = 57% Analysis Date = 05/28/16 Pct Recovery = 57% Analysis Date = 05/28/16 Pct Recovery = 57% Analysis Date = 05/23/16 Pct Recovery = 56% Analysis Date = 05/23/16 Pct Recovery = 56% Analysis Date = 05/18/16 Pct Recovery = 56% Analysis Date = 05/18/16 Pct Recovery = 56% Analysis Date = 05/13/16 Pct Recovery = 56% Analysis Date = 05/13/16 Pct Recovery = 56% Analysis Date = 05/08/16 Pct Recovery = 56% Analysis Date = 05/08/16 Pct Recovery = 56% Analysis Date = 05/03/16 Pct Recovery = 56% Analysis Date = 05/03/16 Pct Recovery = 56% Analysis Date = 04/28/16 Pct Recovery = 56% Analysis Date = 04/28/16 Pct Recovery = 56% Analysis Date = 04/23/16 Pct Recovery = 56% Analysis Date = 04/23/16 Pct Recovery = 56% Analysis Date = 04/18/16 Pct Recovery = 56% Analysis Date = 04/18/16 Pct Recovery = 56% Analysis Date = 04/13/16 Pct Recovery = 56% Analysis Date = 04/13/16 Pct Recovery = 56% Analysis Date = 04/08/16 Pct Recovery = 56% Analysis Date = 04/08/16 Pct Recovery = 56% Analysis Date = 04/03/16 Pct Recovery = 56% Analysis Date = 04/03/16 Pct Recovery = 56% Analysis Date = 03/29/16 Pct Recovery = 56% Analysis Date = 03/29/16 Pct Recovery = 56% Analysis Date = 03/24/16 Pct Recovery = 56% Analysis Date = 03/24/16 Pct Recovery = 56% Analysis Date = 03/19/16 Pct Recovery = 56% Analysis Date = 03/19/16 Pct Recovery = 56% Analysis Date = 03/14/16 Pct Recovery = 56% Analysis Date = 03/14/16 Pct Recovery = 56% Analysis Date = 03/09/16 Pct Recovery = 56% Analysis Date = 03/09/16 Pct Recovery = 56% Analysis Date = 03/04/16 Pct Recovery = 56% Analysis Date = 03/04/16 Pct Recovery = 56% Analysis Date = 02/28/16 Pct Recovery = 56% Analysis Date = 02/28/16 Pct Recovery = 56% Analysis Date = 02/23/16 Pct Recovery = 56% Analysis Date = 02/23/16 Pct Recovery = 56% Analysis Date = 02/18/16 Pct Recovery = 56% Analysis Date = 02/18/16 Pct Recovery = 56% Analysis Date = 02/13/16 Pct Recovery = 56% Analysis Date = 02/13/16 Pct Recovery = 56% Analysis Date = 02/08/16 Pct Recovery = 56% Analysis Date = 02/08/16 Pct Recovery = 56% Analysis Date = 02/03/16 Pct Recovery = 56% Analysis Date = 02/03/16 Pct Recovery = 56% Analysis Date = 01/29/16 Pct Recovery = 56% Analysis Date = 01/29/16 Pct Recovery = 56% Analysis Date = 01/24/16 Pct Recovery = 56% Analysis Date = 01/24/16 Pct Recovery = 56% Analysis Date = 01/19/16 Pct Recovery = 56% Analysis Date = 01/19/16 Pct Recovery = 56% Analysis Date = 01/14/16 Pct Recovery = 56% Analysis Date = 01/14/16 Pct Recovery = 56% Analysis Date = 01/09/16 Pct Recovery = 56% Analysis Date = 01/09/16 Pct Recovery = 56% Analysis Date = 01/04/16 Pct Recovery = 56% Analysis Date = 01/04/16 Pct Recovery = 56% Analysis Date = 12/30/15 Pct Recovery = 56% Analysis Date = 12/30/15 Pct Recovery = 56% Analysis Date = 12/25/15 Pct Recovery = 57% Analysis Date = 12/25/15 Pct Recovery = 57% Analysis Date = 12/20/15 Pct Recovery = 57% Analysis Date = 12/20/15 Pct Recovery = 57% Analysis Date = 12/15/15 Pct Recovery = 57% Analysis Date = 12/15/15 Pct Recovery = 57% Analysis Date = 12/10/15 Pct Recovery = 57% Analysis Date = 12/10/15 Pct Recovery = 57% Analysis Date = 12/05/15 Pct Recovery = 57% Analysis Date = 12/05/15 Pct Recovery = 57% Analysis Date = 11/30/15 Pct Recovery = 57% Analysis Date = 11/30/15 Pct Recovery = 57% Analysis Date = 11/25/15 Pct Recovery = 57% Analysis Date = 11/25/15 Pct Recovery = 57% Analysis Date = 11/20/15 Pct Recovery = 57% Analysis Date = 11/20/15 Pct Recovery = 57% Analysis Date = 11/15/15 Pct Recovery = 58% Analysis Date = 11/15/15 Pct Recovery = 58% Analysis Date = 11/10/15 Pct Recovery = 58% Analysis Date = 11/10/15 Pct Recovery = 58% Analysis Date = 11/05/15 Pct Recovery = 58% Analysis Date = 11/05/15 Pct Recovery = 58% Analysis Date = 10/31/15 Pct Recovery = 58% Analysis Date = 10/31/15 Pct Recovery = 58% Analysis Date = 10/26/15 Pct Recovery = 58% Analysis Date = 10/26/15 Pct Recovery = 58% Analysis Date = 10/21/15 Pct Recovery = 58% Analysis Date = 10/21/15 Pct Recovery = 58% Analysis Date = 10/16/15 Pct Recovery = 58% Analysis Date = 10/16/15 Pct Recovery = 58% Analysis Date = 10/11/15 Pct Recovery = 59% Analysis Date = 10/11/15 Pct Recovery = 59% Analysis Date = 10/06/15 Pct Recovery = 59% Analysis Date = 10/06/15 Pct Recovery = 59% Analysis Date = 10/01/15 Pct Recovery = 59% Analysis Date = 10/01/15 Pct Recovery = 59% Analysis Date = 09/26/15 Pct Recovery = 59% Analysis Date = 09/26/15 Pct Recovery = 59% Analysis Date = 09/21/15 Pct Recovery = 59% Analysis Date = 09/21/15 Pct Recovery = 59% Analysis Date = 09/16/15 Pct Recovery = 59% Analysis Date = 09/16/15 Pct Recovery = 59% Analysis Date = 09/11/15 Pct Recovery = 60% Analysis Date = 09/11/15 Pct Recovery = 60% Analysis Date = 09/05/15 Pct Recovery = 60% Analysis Date = 09/05/15 Pct Recovery = 60% Analysis Date = 08/31/15 Pct Recovery = 60% Analysis Date = 08/31/15 Pct Recovery = 60% Analysis Date = 08/26/15 Pct Recovery = 60% Analysis Date = 08/26/15 Pct Recovery = 60% Analysis Date = 08/21/15 Pct Recovery = 60% Analysis Date = 08/21/15 Pct Recovery = 60% Analysis Date = 08/16/15 Pct Recovery = 60% Analysis Date = 08/16/15 Pct Recovery = 60% Analysis Date = 08/11/15 Pct Recovery = 60% Analysis Date = 08/11/15 Pct Recovery = 60% Analysis Date = 08/06/15 Pct Recovery = 61% Analysis Date = 08/06/15 Pct Recovery = 61% Analysis Date = 08/01/15 Pct Recovery = 61% Analysis Date = 08/01/15 Pct Recovery = 61% Analysis Date = 07/27/15 Pct Recovery = 61% Analysis Date = 07/27/15 Pct Recovery = 61% Analysis Date = 07/22/15 Pct Recovery = 61% Analysis Date = 07/22/15 Pct Recovery = 61% Analysis Date = 07/17/15 Pct Recovery = 61% Analysis Date = 07/17/15 Pct Recovery = 61% Analysis Date = 07/12/15 Pct Recovery = 61% Analysis Date = 07/12/15 Pct Recovery = 61% Analysis Date = 07/07/15 Pct Recovery = 61% Analysis Date = 07/07/15 Pct Recovery = 61% Analysis Date = 07/02/15 Pct Recovery = 62% Analysis Date = 07/02/15 Pct Recovery = 62% Analysis Date = 06/27/15 Pct Recovery = 62% Analysis Date = 06/27/15 Pct Recovery = 62% Analysis Date = 06/22/15 Pct Recovery = 62% Analysis Date = 06/22/15 Pct Recovery = 62% Analysis Date = 06/17/15 Pct Recovery = 62% Analysis Date = 06/17/15 Pct Recovery = 62% Analysis Date = 06/12/15 Pct Recovery = 62% Analysis Date = 06/12/15 Pct Recovery = 62% Analysis Date = 06/07/15 Pct Recovery = 62% Analysis Date = 06/07/15 Pct Recovery = 62% Analysis Date = 06/02/15 Pct Recovery = 62% Analysis Date = 06/02/15 Pct Recovery = 62% Analysis Date = 05/28/15 Pct Recovery = 63% Analysis Date = 05/28/15 Pct Recovery = 63% Analysis Date = 05/23/15 Pct Recovery = 63% Analysis Date = 05/23/15 Pct Recovery = 63% Analysis Date = 05/18/15 Pct Recovery = 63% Analysis Date = 05/18/15 Pct Recovery = 63% Analysis Date = 05/13/15 Pct Recovery = 63% Analysis Date = 05/13/15 Pct Recovery = 63% Analysis Date = 05/08/15 Pct Recovery = 63% Analysis Date = 05/08/15 Pct Recovery = 63% Analysis Date = 05/03/15 Pct Recovery = 63% Analysis Date = 05/03/15 Pct Recovery = 63% Analysis Date = 04/28/15 Pct Recovery = 63% Analysis Date = 04/28/15 Pct Recovery = 63% Analysis Date = 04/23/15 Pct Recovery = 64% Analysis Date = 04/23/15 Pct Recovery = 64% Analysis Date = 04/18/15 Pct Recovery = 64% Analysis Date = 04/18/15 Pct Recovery = 64% Analysis Date = 04/13/15 Pct Recovery = 64% Analysis Date = 04/13/15 Pct Recovery = 64% Analysis Date = 04/08/15 Pct Recovery = 64% Analysis Date = 04/08/15 Pct Recovery = 64% Analysis Date = 04/03/15 Pct Recovery = 64% Analysis Date = 04/03/15 Pct Recovery = 64% Analysis Date = 03/29/15 Pct Recovery = 64% Analysis Date = 03/29/15 Pct Recovery = 64% Analysis Date = 03/24/15 Pct Recovery = 64% Analysis Date = 03/24/15 Pct Recovery = 64% Analysis Date = 03/19/15 Pct Recovery = 65% Analysis Date = 03/19/15 Pct Recovery = 65% Analysis Date = 03/14/15 Pct Recovery = 65% Analysis Date = 03/14/15 Pct Recovery = 65% Analysis Date = 03/09/15 Pct Recovery = 65% Analysis Date = 03/09/15 Pct Recovery = 65% Analysis Date = 03/04/15 Pct Recovery = 65% Analysis Date = 03/04/15 Pct Recovery = 65% Analysis Date = 02/27/15 Pct Recovery = 65% Analysis Date = 02/27/15 Pct Recovery = 65% Analysis Date = 02/22/15 Pct Recovery = 65% Analysis Date = 02/22/15 Pct Recovery = 65% Analysis Date = 02/17/15 Pct Recovery = 65% Analysis Date = 02/17/15 Pct Recovery = 65% Analysis Date = 02/12/15 Pct Recovery = 65% Analysis Date = 02/12/15 Pct Recovery = 65% Analysis Date = 02/07/15 Pct Recovery = 65% Analysis Date = 02/07/15 Pct Recovery = 65% Analysis Date = 02/02/15 Pct Recovery = 65% Analysis Date = 02/02/15 Pct Recovery = 65% Analysis Date = 01/28/15 Pct Recovery = 65% Analysis Date = 01/28/15 Pct Recovery = 65% Analysis Date = 01/23/15 Pct Recovery = 65% Analysis Date = 01/23/15 Pct Recovery = 65% Analysis Date = 01/18/15 Pct Recovery = 64% Analysis Date = 01/18/15 Pct Recovery = 64% Analysis Date = 01/13/15 Pct Recovery = 64% Analysis Date = 01/13/15 Pct Recovery = 64% Analysis Date = 01/08/15 Pct Recovery = 64% Analysis Date = 01/08/15 Pct Recovery = 64% Analysis Date = 01/03/15 Pct Recovery = 64% Analysis Date = 01/03/15 Pct Recovery = 64% Analysis Date = 12/29/14 Pct Recovery = 64% Analysis Date = 12/29/14 Pct Recovery = 64% Analysis Date = 12/24/14 Pct Recovery = 64% Analysis Date = 12/24/14 Pct Recovery = 64% Analysis Date = 12/19/14 Pct Recovery = 64% Analysis Date = 12/19/14 Pct Recovery = 64% Analysis Date = 12/14/14 Pct Recovery = 64% Analysis Date = 12/14/14 Pct Recovery = 64% Analysis Date = 12/09/14 Pct Recovery = 64% Analysis Date = 12/09/14 Pct Recovery = 64% Analysis Date = 12/04/14 Pct Recovery = 64% Analysis Date = 12/04/14 Pct Recovery = 64% Analysis Date = 11/29/14 Pct Recovery = 64% Analysis Date = 11/29/14 Pct Recovery = 64% Analysis Date = 11/24/14 Pct Recovery = 64% Analysis Date = 11/24/14 Pct Recovery = 64% Analysis Date = 11/19/14 Pct Recovery = 64% Analysis Date = 11/19/14 Pct Recovery = 64% Analysis Date = 11/14/14 Pct Recovery = 64% Analysis Date = 11/14/14 Pct Recovery = 64% Analysis Date = 11/09/14 Pct Recovery = 64% Analysis Date = 11/09/14 Pct Recovery = 64% Analysis Date = 11/04/14 Pct Recovery = 64% Analysis Date = 11/04/14 Pct Recovery = 64% Analysis Date = 10/30/14 Pct Recovery = 64% Analysis Date = 10/30/14 Pct Recovery = 64% Analysis Date = 10/25/14 Pct Recovery = 64% Analysis Date = 10/25/14 Pct Recovery = 64% Analysis Date = 10/20/14 Pct Recovery = 63% Analysis Date = 10/20/14 Pct Recovery = 63% Analysis Date = 10/15/14 Pct Recovery = 63% Analysis Date = 10/15/14 Pct Recovery = 63% Analysis Date = 10/10/14 Pct Recovery = 63% Analysis Date = 10/10/14 Pct Recovery = 63% Analysis Date = 10/05/14 Pct Recovery = 63% Analysis Date = 10/05/14 Pct Recovery = 63% Analysis Date = 09/30/14 Pct Recovery = 63% Analysis Date = 09/30/14 Pct Recovery = 63% Analysis Date = 09/25/14 Pct Recovery = 63% Analysis Date = 09/25/14 Pct Recovery = 63% Analysis Date = 09/20/14 Pct Recovery = 63% Analysis Date = 09/20/14 Pct Recovery = 63% Analysis Date = 09/15/14 Pct Recovery = 63% Analysis Date = 09/15/14 Pct Recovery = 63% Analysis Date = 09/10/14 Pct Recovery = 63% Analysis Date = 09/10/14 Pct Recovery = 63% Analysis Date = 09/05/14 Pct Recovery = 63% Analysis Date = 09/05/14 Pct Recovery = 63% Analysis Date = 08/31/14 Pct Recovery = 63% Analysis Date = 08/31/14 Pct Recovery = 63% Analysis Date = 08/26/14 Pct Recovery = 63% Analysis Date = 08/26/14 Pct Recovery = 63% Analysis Date = 08/21/14 Pct Recovery = 63% Analysis Date = 08/21/14 Pct Recovery = 63% Analysis Date = 08/16/14 Pct Recovery = 63% Analysis Date = 08/16/14 Pct Recovery = 63% Analysis Date = 08/11/14 Pct Recovery = 62% Analysis Date = 08/11/14 Pct Recovery = 62% Analysis Date = 08/06/14 Pct Recovery = 62% Analysis Date = 08/06/14 Pct Recovery = 62% Analysis Date = 08/01/14 Pct Recovery = 62% Analysis Date = 08/01/14 Pct Recovery = 62% Analysis Date = 07/27/14 Pct Recovery = 62% Analysis Date = 07/27/14 Pct Recovery = 62% Analysis Date = 07/22/14 Pct Recovery = 62% Analysis Date = 07/22/14 Pct Recovery = 62% Analysis Date = 07/17/14 Pct Recovery = 62% Analysis Date = 07/17/14 Pct Recovery = 62% Analysis Date = 07/12/14 Pct Recovery = 62% Analysis Date = 07/12/14 Pct Recovery = 62% Analysis Date = 07/07/14 Pct Recovery = 62% Analysis Date = 07/07/14 Pct Recovery = 62% Analysis Date = 07/02/14 Pct Recovery = 62% Analysis Date = 07/02/14 Pct Recovery = 62% Analysis Date = 06/27/14 Pct Recovery = 62% Analysis Date = 06/27/14 Pct Recovery = 62% Analysis Date = 06/22/14 Pct Recovery = 62% Analysis Date = 06/22/14 Pct Recovery = 62% Analysis Date = 06/17/14 Pct Recovery = 61% Analysis Date = 06/17/14 Pct Recovery = 61% Analysis Date = 06/12/14 Pct Recovery = 61% Analysis Date = 06/12/14 Pct Recovery = 61% Analysis Date = 06/07/14 Pct Recovery = 61% Analysis Date = 06/07/14 Pct Recovery = 61% Analysis Date = 06/02/14 Pct Recovery = 61% Analysis Date = 06/02/14 Pct Recovery = 61% Analysis Date = 05/28/14 Pct Recovery = 61% Analysis Date = 05/28/14 Pct Recovery = 61% Analysis Date = 05/23/14 Pct Recovery = 61% Analysis Date = 05/23/14 Pct Recovery = 61% Analysis Date = 05/18/14 Pct Recovery = 61% Analysis Date = 05/18/14 Pct Recovery = 61% Analysis Date = 05/13/14 Pct Recovery = 61% Analysis Date = 05/13/14 Pct Recovery = 61% Analysis Date = 05/08/14 Pct Recovery = 61% Analysis Date = 05/08/14 Pct Recovery = 61% Analysis Date = 05/03/14 Pct Recovery = 61% Analysis Date = 05/03/14 Pct Recovery = 61% Analysis Date = 04/28/14 Pct Recovery = 60% Analysis Date = 04/28/14 Pct Recovery = 60% Analysis Date = 04/23/14 Pct Recovery = 60% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
NORFLUOXETINE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 69 60% 14% 58% 15%
Total 69 60% 14% 58% 15%

Sample Statistics
NORFLUOXETINE

Characteristic N % % Basis
Plotted 69 100% Spiked
Estimated Values 65 94% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 69 .  
False Negatives 0 0% 0 out of 69
Not Spiked 46 .  
False Positives 0 0% 0 out of 46

BQS OBSP Determination:
NORSERTRALINE
METHOD: 2440 , TESTIDCODE: 67532LCM56
Open Data Set

Analysis Date = 11/05/15 SpikeMix = ERA 0406-15-08: 80 µl & Abs 052215: 80 µl Pct Recovery = 59% Analysis Date = 11/04/15 SpikeMix = Abs 052215: 80 µl & Abs 050115: 80 µl Pct Recovery = 45% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 51% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 52% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 49% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 46% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-08: 40 µl & Abs 052215: 40 µl Pct Recovery = 63% Analysis Date = 02/23/16 SpikeMix = Abs 052215: 40 µl & Abs 050115: 40 µl Pct Recovery = 61% Analysis Date = 09/10/15 SpikeMix = Abs 052215: 40 µl & ERA 0406-15-07A: 40 µl Pct Recovery = 69% Analysis Date = 07/31/15 SpikeMix = Abs 051315: 40 µl & Abs 052215: 40 µl Pct Recovery = 89% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 68% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 64% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 52% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 52% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 37% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 35% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 37% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 44% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 53% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 48% Analysis Date = 02/23/16 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 54% Analysis Date = 11/24/15 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 48% Analysis Date = 09/09/15 SpikeMix = ERA 0406-15-08: 20 µl & Abs 052215: 20 µl Pct Recovery = 48% Analysis Date = 08/27/15 SpikeMix = Abs 052215: 20 µl & Abs 050115: 20 µl Pct Recovery = 40% Analysis Date = 07/09/15 SpikeMix = Abs 050115: 20 µl & Abs 052215: 20 µl Pct Recovery = 54% Analysis Date = 06/26/15 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 49% Analysis Date = 10/28/16 Pct Recovery = 59% Analysis Date = 10/25/16 Pct Recovery = 58% Analysis Date = 10/25/16 Pct Recovery = 58% Analysis Date = 10/23/16 Pct Recovery = 58% Analysis Date = 10/23/16 Pct Recovery = 58% Analysis Date = 10/20/16 Pct Recovery = 57% Analysis Date = 10/20/16 Pct Recovery = 57% Analysis Date = 10/18/16 Pct Recovery = 57% Analysis Date = 10/18/16 Pct Recovery = 57% Analysis Date = 10/15/16 Pct Recovery = 56% Analysis Date = 10/15/16 Pct Recovery = 56% Analysis Date = 10/13/16 Pct Recovery = 56% Analysis Date = 10/13/16 Pct Recovery = 56% Analysis Date = 10/10/16 Pct Recovery = 56% Analysis Date = 10/10/16 Pct Recovery = 56% Analysis Date = 10/08/16 Pct Recovery = 55% Analysis Date = 10/08/16 Pct Recovery = 55% Analysis Date = 10/05/16 Pct Recovery = 55% Analysis Date = 10/05/16 Pct Recovery = 55% Analysis Date = 10/03/16 Pct Recovery = 54% Analysis Date = 10/03/16 Pct Recovery = 54% Analysis Date = 10/01/16 Pct Recovery = 54% Analysis Date = 10/01/16 Pct Recovery = 54% Analysis Date = 09/28/16 Pct Recovery = 54% Analysis Date = 09/28/16 Pct Recovery = 54% Analysis Date = 09/26/16 Pct Recovery = 53% Analysis Date = 09/26/16 Pct Recovery = 53% Analysis Date = 09/23/16 Pct Recovery = 53% Analysis Date = 09/23/16 Pct Recovery = 53% Analysis Date = 09/21/16 Pct Recovery = 52% Analysis Date = 09/21/16 Pct Recovery = 52% Analysis Date = 09/18/16 Pct Recovery = 52% Analysis Date = 09/18/16 Pct Recovery = 52% Analysis Date = 09/16/16 Pct Recovery = 52% Analysis Date = 09/16/16 Pct Recovery = 52% Analysis Date = 09/13/16 Pct Recovery = 51% Analysis Date = 09/13/16 Pct Recovery = 51% Analysis Date = 09/11/16 Pct Recovery = 51% Analysis Date = 09/11/16 Pct Recovery = 51% Analysis Date = 09/09/16 Pct Recovery = 51% Analysis Date = 09/09/16 Pct Recovery = 51% Analysis Date = 09/06/16 Pct Recovery = 51% Analysis Date = 09/06/16 Pct Recovery = 51% Analysis Date = 09/04/16 Pct Recovery = 50% Analysis Date = 09/04/16 Pct Recovery = 50% Analysis Date = 09/01/16 Pct Recovery = 50% Analysis Date = 09/01/16 Pct Recovery = 50% Analysis Date = 08/30/16 Pct Recovery = 50% Analysis Date = 08/30/16 Pct Recovery = 50% Analysis Date = 08/27/16 Pct Recovery = 49% Analysis Date = 08/27/16 Pct Recovery = 49% Analysis Date = 08/25/16 Pct Recovery = 49% Analysis Date = 08/25/16 Pct Recovery = 49% Analysis Date = 08/22/16 Pct Recovery = 49% Analysis Date = 08/22/16 Pct Recovery = 49% Analysis Date = 08/20/16 Pct Recovery = 48% Analysis Date = 08/20/16 Pct Recovery = 48% Analysis Date = 08/17/16 Pct Recovery = 48% Analysis Date = 08/17/16 Pct Recovery = 48% Analysis Date = 08/15/16 Pct Recovery = 48% Analysis Date = 08/15/16 Pct Recovery = 48% Analysis Date = 08/13/16 Pct Recovery = 47% Analysis Date = 08/13/16 Pct Recovery = 47% Analysis Date = 08/10/16 Pct Recovery = 47% Analysis Date = 08/10/16 Pct Recovery = 47% Analysis Date = 08/08/16 Pct Recovery = 47% Analysis Date = 08/08/16 Pct Recovery = 47% Analysis Date = 08/05/16 Pct Recovery = 47% Analysis Date = 08/05/16 Pct Recovery = 47% Analysis Date = 08/03/16 Pct Recovery = 47% Analysis Date = 08/03/16 Pct Recovery = 47% Analysis Date = 07/31/16 Pct Recovery = 46% Analysis Date = 07/31/16 Pct Recovery = 46% Analysis Date = 07/29/16 Pct Recovery = 46% Analysis Date = 07/29/16 Pct Recovery = 46% Analysis Date = 07/26/16 Pct Recovery = 46% Analysis Date = 07/26/16 Pct Recovery = 46% Analysis Date = 07/24/16 Pct Recovery = 46% Analysis Date = 07/24/16 Pct Recovery = 46% Analysis Date = 07/22/16 Pct Recovery = 46% Analysis Date = 07/22/16 Pct Recovery = 46% Analysis Date = 07/19/16 Pct Recovery = 46% Analysis Date = 07/19/16 Pct Recovery = 46% Analysis Date = 07/17/16 Pct Recovery = 46% Analysis Date = 07/17/16 Pct Recovery = 46% Analysis Date = 07/14/16 Pct Recovery = 46% Analysis Date = 07/14/16 Pct Recovery = 46% Analysis Date = 07/12/16 Pct Recovery = 47% Analysis Date = 07/12/16 Pct Recovery = 47% Analysis Date = 07/09/16 Pct Recovery = 47% Analysis Date = 07/09/16 Pct Recovery = 47% Analysis Date = 07/07/16 Pct Recovery = 47% Analysis Date = 07/07/16 Pct Recovery = 47% Analysis Date = 07/04/16 Pct Recovery = 47% Analysis Date = 07/04/16 Pct Recovery = 47% Analysis Date = 07/02/16 Pct Recovery = 47% Analysis Date = 07/02/16 Pct Recovery = 47% Analysis Date = 06/29/16 Pct Recovery = 48% Analysis Date = 06/29/16 Pct Recovery = 48% Analysis Date = 06/27/16 Pct Recovery = 48% Analysis Date = 06/27/16 Pct Recovery = 48% Analysis Date = 06/25/16 Pct Recovery = 48% Analysis Date = 06/25/16 Pct Recovery = 48% Analysis Date = 06/22/16 Pct Recovery = 48% Analysis Date = 06/22/16 Pct Recovery = 48% Analysis Date = 06/20/16 Pct Recovery = 48% Analysis Date = 06/20/16 Pct Recovery = 48% Analysis Date = 06/17/16 Pct Recovery = 49% Analysis Date = 06/17/16 Pct Recovery = 49% Analysis Date = 06/15/16 Pct Recovery = 49% Analysis Date = 06/15/16 Pct Recovery = 49% Analysis Date = 06/12/16 Pct Recovery = 49% Analysis Date = 06/12/16 Pct Recovery = 49% Analysis Date = 06/10/16 Pct Recovery = 49% Analysis Date = 06/10/16 Pct Recovery = 49% Analysis Date = 06/07/16 Pct Recovery = 49% Analysis Date = 06/07/16 Pct Recovery = 49% Analysis Date = 06/05/16 Pct Recovery = 50% Analysis Date = 06/05/16 Pct Recovery = 50% Analysis Date = 06/03/16 Pct Recovery = 50% Analysis Date = 06/03/16 Pct Recovery = 50% Analysis Date = 05/31/16 Pct Recovery = 50% Analysis Date = 05/31/16 Pct Recovery = 50% Analysis Date = 05/29/16 Pct Recovery = 50% Analysis Date = 05/29/16 Pct Recovery = 50% Analysis Date = 05/26/16 Pct Recovery = 50% Analysis Date = 05/26/16 Pct Recovery = 50% Analysis Date = 05/24/16 Pct Recovery = 50% Analysis Date = 05/24/16 Pct Recovery = 50% Analysis Date = 05/21/16 Pct Recovery = 51% Analysis Date = 05/21/16 Pct Recovery = 51% Analysis Date = 05/19/16 Pct Recovery = 51% Analysis Date = 05/19/16 Pct Recovery = 51% Analysis Date = 05/16/16 Pct Recovery = 51% Analysis Date = 05/16/16 Pct Recovery = 51% Analysis Date = 05/14/16 Pct Recovery = 51% Analysis Date = 05/14/16 Pct Recovery = 51% Analysis Date = 05/11/16 Pct Recovery = 51% Analysis Date = 05/11/16 Pct Recovery = 51% Analysis Date = 05/09/16 Pct Recovery = 52% Analysis Date = 05/09/16 Pct Recovery = 52% Analysis Date = 05/07/16 Pct Recovery = 52% Analysis Date = 05/07/16 Pct Recovery = 52% Analysis Date = 05/04/16 Pct Recovery = 52% Analysis Date = 05/04/16 Pct Recovery = 52% Analysis Date = 05/02/16 Pct Recovery = 52% Analysis Date = 05/02/16 Pct Recovery = 52% Analysis Date = 04/29/16 Pct Recovery = 52% Analysis Date = 04/29/16 Pct Recovery = 52% Analysis Date = 04/27/16 Pct Recovery = 52% Analysis Date = 04/27/16 Pct Recovery = 52% Analysis Date = 04/24/16 Pct Recovery = 52% Analysis Date = 04/24/16 Pct Recovery = 52% Analysis Date = 04/22/16 Pct Recovery = 52% Analysis Date = 04/22/16 Pct Recovery = 52% Analysis Date = 04/19/16 Pct Recovery = 52% Analysis Date = 04/19/16 Pct Recovery = 52% Analysis Date = 04/17/16 Pct Recovery = 53% Analysis Date = 04/17/16 Pct Recovery = 53% Analysis Date = 04/15/16 Pct Recovery = 53% Analysis Date = 04/15/16 Pct Recovery = 53% Analysis Date = 04/12/16 Pct Recovery = 53% Analysis Date = 04/12/16 Pct Recovery = 53% Analysis Date = 04/10/16 Pct Recovery = 53% Analysis Date = 04/10/16 Pct Recovery = 53% Analysis Date = 04/07/16 Pct Recovery = 53% Analysis Date = 04/07/16 Pct Recovery = 53% Analysis Date = 04/05/16 Pct Recovery = 53% Analysis Date = 04/05/16 Pct Recovery = 53% Analysis Date = 04/02/16 Pct Recovery = 53% Analysis Date = 04/02/16 Pct Recovery = 53% Analysis Date = 03/31/16 Pct Recovery = 53% Analysis Date = 03/31/16 Pct Recovery = 53% Analysis Date = 03/28/16 Pct Recovery = 53% Analysis Date = 03/28/16 Pct Recovery = 53% Analysis Date = 03/26/16 Pct Recovery = 53% Analysis Date = 03/26/16 Pct Recovery = 53% Analysis Date = 03/23/16 Pct Recovery = 54% Analysis Date = 03/23/16 Pct Recovery = 54% Analysis Date = 03/21/16 Pct Recovery = 54% Analysis Date = 03/21/16 Pct Recovery = 54% Analysis Date = 03/19/16 Pct Recovery = 54% Analysis Date = 03/19/16 Pct Recovery = 54% Analysis Date = 03/16/16 Pct Recovery = 54% Analysis Date = 03/16/16 Pct Recovery = 54% Analysis Date = 03/14/16 Pct Recovery = 54% Analysis Date = 03/14/16 Pct Recovery = 54% Analysis Date = 03/11/16 Pct Recovery = 54% Analysis Date = 03/11/16 Pct Recovery = 54% Analysis Date = 03/09/16 Pct Recovery = 54% Analysis Date = 03/09/16 Pct Recovery = 54% Analysis Date = 03/06/16 Pct Recovery = 54% Analysis Date = 03/06/16 Pct Recovery = 54% Analysis Date = 03/04/16 Pct Recovery = 54% Analysis Date = 03/04/16 Pct Recovery = 54% Analysis Date = 03/01/16 Pct Recovery = 55% Analysis Date = 03/01/16 Pct Recovery = 55% Analysis Date = 02/28/16 Pct Recovery = 55% Analysis Date = 02/28/16 Pct Recovery = 55% Analysis Date = 02/26/16 Pct Recovery = 55% Analysis Date = 02/26/16 Pct Recovery = 55% Analysis Date = 02/23/16 Pct Recovery = 55% Analysis Date = 02/23/16 Pct Recovery = 55% Analysis Date = 02/21/16 Pct Recovery = 55% Analysis Date = 02/21/16 Pct Recovery = 55% Analysis Date = 02/18/16 Pct Recovery = 55% Analysis Date = 02/18/16 Pct Recovery = 55% Analysis Date = 02/16/16 Pct Recovery = 55% Analysis Date = 02/16/16 Pct Recovery = 55% Analysis Date = 02/13/16 Pct Recovery = 55% Analysis Date = 02/13/16 Pct Recovery = 55% Analysis Date = 02/11/16 Pct Recovery = 55% Analysis Date = 02/11/16 Pct Recovery = 55% Analysis Date = 02/08/16 Pct Recovery = 55% Analysis Date = 02/08/16 Pct Recovery = 55% Analysis Date = 02/06/16 Pct Recovery = 55% Analysis Date = 02/06/16 Pct Recovery = 55% Analysis Date = 02/03/16 Pct Recovery = 55% Analysis Date = 02/03/16 Pct Recovery = 55% Analysis Date = 02/01/16 Pct Recovery = 55% Analysis Date = 02/01/16 Pct Recovery = 55% Analysis Date = 01/30/16 Pct Recovery = 55% Analysis Date = 01/30/16 Pct Recovery = 55% Analysis Date = 01/27/16 Pct Recovery = 55% Analysis Date = 01/27/16 Pct Recovery = 55% Analysis Date = 01/25/16 Pct Recovery = 55% Analysis Date = 01/25/16 Pct Recovery = 55% Analysis Date = 01/22/16 Pct Recovery = 55% Analysis Date = 01/22/16 Pct Recovery = 55% Analysis Date = 01/20/16 Pct Recovery = 55% Analysis Date = 01/20/16 Pct Recovery = 55% Analysis Date = 01/17/16 Pct Recovery = 55% Analysis Date = 01/17/16 Pct Recovery = 55% Analysis Date = 01/15/16 Pct Recovery = 55% Analysis Date = 01/15/16 Pct Recovery = 55% Analysis Date = 01/12/16 Pct Recovery = 55% Analysis Date = 01/12/16 Pct Recovery = 55% Analysis Date = 01/10/16 Pct Recovery = 55% Analysis Date = 01/10/16 Pct Recovery = 55% Analysis Date = 01/08/16 Pct Recovery = 55% Analysis Date = 01/08/16 Pct Recovery = 55% Analysis Date = 01/05/16 Pct Recovery = 55% Analysis Date = 01/05/16 Pct Recovery = 55% Analysis Date = 01/03/16 Pct Recovery = 55% Analysis Date = 01/03/16 Pct Recovery = 55% Analysis Date = 12/31/15 Pct Recovery = 56% Analysis Date = 12/31/15 Pct Recovery = 56% Analysis Date = 12/29/15 Pct Recovery = 56% Analysis Date = 12/29/15 Pct Recovery = 56% Analysis Date = 12/26/15 Pct Recovery = 56% Analysis Date = 12/26/15 Pct Recovery = 56% Analysis Date = 12/24/15 Pct Recovery = 56% Analysis Date = 12/24/15 Pct Recovery = 56% Analysis Date = 12/21/15 Pct Recovery = 56% Analysis Date = 12/21/15 Pct Recovery = 56% Analysis Date = 12/19/15 Pct Recovery = 56% Analysis Date = 12/19/15 Pct Recovery = 56% Analysis Date = 12/16/15 Pct Recovery = 56% Analysis Date = 12/16/15 Pct Recovery = 56% Analysis Date = 12/14/15 Pct Recovery = 56% Analysis Date = 12/14/15 Pct Recovery = 56% Analysis Date = 12/12/15 Pct Recovery = 56% Analysis Date = 12/12/15 Pct Recovery = 56% Analysis Date = 12/09/15 Pct Recovery = 56% Analysis Date = 12/09/15 Pct Recovery = 56% Analysis Date = 12/07/15 Pct Recovery = 56% Analysis Date = 12/07/15 Pct Recovery = 56% Analysis Date = 12/04/15 Pct Recovery = 56% Analysis Date = 12/04/15 Pct Recovery = 56% Analysis Date = 12/02/15 Pct Recovery = 56% Analysis Date = 12/02/15 Pct Recovery = 56% Analysis Date = 11/29/15 Pct Recovery = 56% Analysis Date = 11/29/15 Pct Recovery = 56% Analysis Date = 11/27/15 Pct Recovery = 56% Analysis Date = 11/27/15 Pct Recovery = 56% Analysis Date = 11/24/15 Pct Recovery = 56% Analysis Date = 11/24/15 Pct Recovery = 56% Analysis Date = 11/22/15 Pct Recovery = 56% Analysis Date = 11/22/15 Pct Recovery = 56% Analysis Date = 11/20/15 Pct Recovery = 56% Analysis Date = 11/20/15 Pct Recovery = 56% Analysis Date = 11/17/15 Pct Recovery = 56% Analysis Date = 11/17/15 Pct Recovery = 56% Analysis Date = 11/15/15 Pct Recovery = 56% Analysis Date = 11/15/15 Pct Recovery = 56% Analysis Date = 11/12/15 Pct Recovery = 56% Analysis Date = 11/12/15 Pct Recovery = 56% Analysis Date = 11/10/15 Pct Recovery = 56% Analysis Date = 11/10/15 Pct Recovery = 56% Analysis Date = 11/07/15 Pct Recovery = 56% Analysis Date = 11/07/15 Pct Recovery = 56% Analysis Date = 11/05/15 Pct Recovery = 56% Analysis Date = 11/05/15 Pct Recovery = 56% Analysis Date = 11/02/15 Pct Recovery = 56% Analysis Date = 11/02/15 Pct Recovery = 56% Analysis Date = 10/31/15 Pct Recovery = 56% Analysis Date = 10/31/15 Pct Recovery = 56% Analysis Date = 10/28/15 Pct Recovery = 56% Analysis Date = 10/28/15 Pct Recovery = 56% Analysis Date = 10/26/15 Pct Recovery = 56% Analysis Date = 10/26/15 Pct Recovery = 56% Analysis Date = 10/24/15 Pct Recovery = 56% Analysis Date = 10/24/15 Pct Recovery = 56% Analysis Date = 10/21/15 Pct Recovery = 56% Analysis Date = 10/21/15 Pct Recovery = 56% Analysis Date = 10/19/15 Pct Recovery = 56% Analysis Date = 10/19/15 Pct Recovery = 56% Analysis Date = 10/16/15 Pct Recovery = 56% Analysis Date = 10/16/15 Pct Recovery = 56% Analysis Date = 10/14/15 Pct Recovery = 56% Analysis Date = 10/14/15 Pct Recovery = 56% Analysis Date = 10/11/15 Pct Recovery = 56% Analysis Date = 10/11/15 Pct Recovery = 56% Analysis Date = 10/09/15 Pct Recovery = 56% Analysis Date = 10/09/15 Pct Recovery = 56% Analysis Date = 10/06/15 Pct Recovery = 56% Analysis Date = 10/06/15 Pct Recovery = 56% Analysis Date = 10/04/15 Pct Recovery = 56% Analysis Date = 10/04/15 Pct Recovery = 56% Analysis Date = 10/02/15 Pct Recovery = 57% Analysis Date = 10/02/15 Pct Recovery = 57% Analysis Date = 09/29/15 Pct Recovery = 57% Analysis Date = 09/29/15 Pct Recovery = 57% Analysis Date = 09/27/15 Pct Recovery = 57% Analysis Date = 09/27/15 Pct Recovery = 57% Analysis Date = 09/24/15 Pct Recovery = 57% Analysis Date = 09/24/15 Pct Recovery = 57% Analysis Date = 09/22/15 Pct Recovery = 57% Analysis Date = 09/22/15 Pct Recovery = 57% Analysis Date = 09/19/15 Pct Recovery = 57% Analysis Date = 09/19/15 Pct Recovery = 57% Analysis Date = 09/17/15 Pct Recovery = 57% Analysis Date = 09/17/15 Pct Recovery = 57% Analysis Date = 09/14/15 Pct Recovery = 57% Analysis Date = 09/14/15 Pct Recovery = 57% Analysis Date = 09/12/15 Pct Recovery = 57% Analysis Date = 09/12/15 Pct Recovery = 57% Analysis Date = 09/09/15 Pct Recovery = 57% Analysis Date = 09/09/15 Pct Recovery = 57% Analysis Date = 09/07/15 Pct Recovery = 57% Analysis Date = 09/07/15 Pct Recovery = 57% Analysis Date = 09/05/15 Pct Recovery = 57% Analysis Date = 09/05/15 Pct Recovery = 57% Analysis Date = 09/02/15 Pct Recovery = 57% Analysis Date = 09/02/15 Pct Recovery = 57% Analysis Date = 08/31/15 Pct Recovery = 57% Analysis Date = 08/31/15 Pct Recovery = 57% Analysis Date = 08/28/15 Pct Recovery = 57% Analysis Date = 08/28/15 Pct Recovery = 57% Analysis Date = 08/26/15 Pct Recovery = 57% Analysis Date = 08/26/15 Pct Recovery = 57% Analysis Date = 08/23/15 Pct Recovery = 57% Analysis Date = 08/23/15 Pct Recovery = 57% Analysis Date = 08/21/15 Pct Recovery = 57% Analysis Date = 08/21/15 Pct Recovery = 57% Analysis Date = 08/18/15 Pct Recovery = 57% Analysis Date = 08/18/15 Pct Recovery = 57% Analysis Date = 08/16/15 Pct Recovery = 57% Analysis Date = 08/16/15 Pct Recovery = 57% Analysis Date = 08/14/15 Pct Recovery = 57% Analysis Date = 08/14/15 Pct Recovery = 57% Analysis Date = 08/11/15 Pct Recovery = 57% Analysis Date = 08/11/15 Pct Recovery = 57% Analysis Date = 08/09/15 Pct Recovery = 57% Analysis Date = 08/09/15 Pct Recovery = 57% Analysis Date = 08/06/15 Pct Recovery = 57% Analysis Date = 08/06/15 Pct Recovery = 57% Analysis Date = 08/04/15 Pct Recovery = 57% Analysis Date = 08/04/15 Pct Recovery = 57% Analysis Date = 08/01/15 Pct Recovery = 57% Analysis Date = 08/01/15 Pct Recovery = 57% Analysis Date = 07/30/15 Pct Recovery = 57% Analysis Date = 07/30/15 Pct Recovery = 57% Analysis Date = 07/27/15 Pct Recovery = 57% Analysis Date = 07/27/15 Pct Recovery = 57% Analysis Date = 07/25/15 Pct Recovery = 57% Analysis Date = 07/25/15 Pct Recovery = 57% Analysis Date = 07/22/15 Pct Recovery = 57% Analysis Date = 07/22/15 Pct Recovery = 57% Analysis Date = 07/20/15 Pct Recovery = 57% Analysis Date = 07/20/15 Pct Recovery = 57% Analysis Date = 07/18/15 Pct Recovery = 57% Analysis Date = 07/18/15 Pct Recovery = 57% Analysis Date = 07/15/15 Pct Recovery = 57% Analysis Date = 07/15/15 Pct Recovery = 57% Analysis Date = 07/13/15 Pct Recovery = 58% Analysis Date = 07/13/15 Pct Recovery = 58% Analysis Date = 07/10/15 Pct Recovery = 58% Analysis Date = 07/10/15 Pct Recovery = 58% Analysis Date = 07/08/15 Pct Recovery = 58% Analysis Date = 07/08/15 Pct Recovery = 58% Analysis Date = 07/05/15 Pct Recovery = 58% Analysis Date = 07/05/15 Pct Recovery = 58% Analysis Date = 07/03/15 Pct Recovery = 58% Analysis Date = 07/03/15 Pct Recovery = 58% Analysis Date = 06/30/15 Pct Recovery = 58% Analysis Date = 06/30/15 Pct Recovery = 58% Analysis Date = 06/28/15 Pct Recovery = 58% Analysis Date = 06/28/15 Pct Recovery = 58% Analysis Date = 06/26/15 Pct Recovery = 58% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
NORSERTRALINE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 26 53% 12% 51% 10%
Total 26 53% 12% 51% 10%

Sample Statistics
NORSERTRALINE

Characteristic N % % Basis
Plotted 26 93% Spiked
Estimated Values 26 93% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 28 .  
False Negatives 2 7% 2 out of 28
Not Spiked 87 .  
False Positives 0 0% 0 out of 87

BQS OBSP Determination:
NORVERAPAMIL
METHOD: 2440 , TESTIDCODE: 68007LCM56
Open Data Set

Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 26% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 35% Analysis Date = 11/24/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 48% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 80 µl & Abs 051315: 80 µl Pct Recovery = 22% Analysis Date = 10/01/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 17% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 80 µl & ERA 0406-15-08: 80 µl Pct Recovery = 58% Analysis Date = 11/05/15 SpikeMix = ERA 0406-15-08: 80 µl & Abs 052215: 80 µl Pct Recovery = 34% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 37% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 45% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 53% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 57% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-04: 15 µl & Abs 041814: 15 µl Pct Recovery = 33% Analysis Date = 02/06/15 SpikeMix = Abs 041814: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 37% Analysis Date = 07/12/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 54% Analysis Date = 06/22/14 SpikeMix = Abs 041814: 60 µl & Abs 041614: 60 µl Pct Recovery = 57% Analysis Date = 05/21/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 53% Analysis Date = 05/07/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 26% Analysis Date = 04/29/15 SpikeMix = ERA 0319-14-05: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 59% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 33% Analysis Date = 01/16/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 38% Analysis Date = 12/07/14 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 46% Analysis Date = 12/06/14 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 46% Analysis Date = 08/28/14 SpikeMix = ERA 0319-14-04: 60 µl & ERA 0319-14-05: 60 µl Pct Recovery = 32% Analysis Date = 07/26/14 SpikeMix = ERA 0319-14-05: 60 µl & ERA 0318-14-02: 60 µl Pct Recovery = 51% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 47% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 40% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-07A: 40 µl & Abs 051315: 40 µl Pct Recovery = 30% Analysis Date = 07/31/15 SpikeMix = Abs 051315: 40 µl & Abs 052215: 40 µl Pct Recovery = 34% Analysis Date = 07/30/15 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 39% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-08: 40 µl & Abs 052215: 40 µl Pct Recovery = 31% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 76% Analysis Date = 11/04/15 SpikeMix = ERA 0406-15-07A: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 38% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 29% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 36% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 21% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 33% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 10% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 29% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 31% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 39% Analysis Date = 11/04/14 SpikeMix = Abs 041814: 8 µl & ERA 0318-14-02: 8 µl Pct Recovery = 9% Analysis Date = 10/11/14 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 13% Analysis Date = 10/10/14 SpikeMix = Abs 041714: 30 µl & Abs 041814: 30 µl Pct Recovery = 29% Analysis Date = 10/10/14 SpikeMix = Abs 041814: 30 µl & ERA 0318-14-02: 30 µl Pct Recovery = 35% Analysis Date = 05/30/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 31% Analysis Date = 04/23/14 SpikeMix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.2: 20 µl Pct Recovery = 45% Analysis Date = 08/30/14 SpikeMix = ERA 0318-14-02: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 47% Analysis Date = 08/16/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 24% Analysis Date = 02/23/16 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 136% Analysis Date = 06/26/15 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 36% Analysis Date = 06/09/15 SpikeMix = Abs 051315: 20 µl & Abs 050115: 20 µl Pct Recovery = 14% Analysis Date = 04/27/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 48% Analysis Date = 11/25/15 SpikeMix = Abs 050115: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 29% Analysis Date = 04/09/16 SpikeMix = Abs 051315: 10 µl & ERA 0406-15-09: 10 µl Pct Recovery = 13% Analysis Date = 01/18/17 Pct Recovery = 27% Analysis Date = 01/13/17 Pct Recovery = 28% Analysis Date = 01/13/17 Pct Recovery = 28% Analysis Date = 01/08/17 Pct Recovery = 28% Analysis Date = 01/08/17 Pct Recovery = 28% Analysis Date = 01/03/17 Pct Recovery = 28% Analysis Date = 01/03/17 Pct Recovery = 28% Analysis Date = 12/29/16 Pct Recovery = 29% Analysis Date = 12/29/16 Pct Recovery = 29% Analysis Date = 12/24/16 Pct Recovery = 29% Analysis Date = 12/24/16 Pct Recovery = 29% Analysis Date = 12/19/16 Pct Recovery = 29% Analysis Date = 12/19/16 Pct Recovery = 29% Analysis Date = 12/14/16 Pct Recovery = 30% Analysis Date = 12/14/16 Pct Recovery = 30% Analysis Date = 12/09/16 Pct Recovery = 30% Analysis Date = 12/09/16 Pct Recovery = 30% Analysis Date = 12/04/16 Pct Recovery = 30% Analysis Date = 12/04/16 Pct Recovery = 30% Analysis Date = 11/29/16 Pct Recovery = 31% Analysis Date = 11/29/16 Pct Recovery = 31% Analysis Date = 11/24/16 Pct Recovery = 31% Analysis Date = 11/24/16 Pct Recovery = 31% Analysis Date = 11/19/16 Pct Recovery = 31% Analysis Date = 11/19/16 Pct Recovery = 31% Analysis Date = 11/14/16 Pct Recovery = 32% Analysis Date = 11/14/16 Pct Recovery = 32% Analysis Date = 11/09/16 Pct Recovery = 32% Analysis Date = 11/09/16 Pct Recovery = 32% Analysis Date = 11/04/16 Pct Recovery = 32% Analysis Date = 11/04/16 Pct Recovery = 32% Analysis Date = 10/30/16 Pct Recovery = 33% Analysis Date = 10/30/16 Pct Recovery = 33% Analysis Date = 10/25/16 Pct Recovery = 33% Analysis Date = 10/25/16 Pct Recovery = 33% Analysis Date = 10/20/16 Pct Recovery = 33% Analysis Date = 10/20/16 Pct Recovery = 33% Analysis Date = 10/15/16 Pct Recovery = 34% Analysis Date = 10/15/16 Pct Recovery = 34% Analysis Date = 10/10/16 Pct Recovery = 34% Analysis Date = 10/10/16 Pct Recovery = 34% Analysis Date = 10/05/16 Pct Recovery = 34% Analysis Date = 10/05/16 Pct Recovery = 34% Analysis Date = 09/30/16 Pct Recovery = 35% Analysis Date = 09/30/16 Pct Recovery = 35% Analysis Date = 09/25/16 Pct Recovery = 35% Analysis Date = 09/25/16 Pct Recovery = 35% Analysis Date = 09/20/16 Pct Recovery = 35% Analysis Date = 09/20/16 Pct Recovery = 35% Analysis Date = 09/15/16 Pct Recovery = 36% Analysis Date = 09/15/16 Pct Recovery = 36% Analysis Date = 09/10/16 Pct Recovery = 36% Analysis Date = 09/10/16 Pct Recovery = 36% Analysis Date = 09/05/16 Pct Recovery = 36% Analysis Date = 09/05/16 Pct Recovery = 36% Analysis Date = 08/31/16 Pct Recovery = 37% Analysis Date = 08/31/16 Pct Recovery = 37% Analysis Date = 08/26/16 Pct Recovery = 37% Analysis Date = 08/26/16 Pct Recovery = 37% Analysis Date = 08/21/16 Pct Recovery = 37% Analysis Date = 08/21/16 Pct Recovery = 37% Analysis Date = 08/16/16 Pct Recovery = 38% Analysis Date = 08/16/16 Pct Recovery = 38% Analysis Date = 08/11/16 Pct Recovery = 38% Analysis Date = 08/11/16 Pct Recovery = 38% Analysis Date = 08/06/16 Pct Recovery = 38% Analysis Date = 08/06/16 Pct Recovery = 38% Analysis Date = 08/01/16 Pct Recovery = 38% Analysis Date = 08/01/16 Pct Recovery = 38% Analysis Date = 07/27/16 Pct Recovery = 39% Analysis Date = 07/27/16 Pct Recovery = 39% Analysis Date = 07/22/16 Pct Recovery = 39% Analysis Date = 07/22/16 Pct Recovery = 39% Analysis Date = 07/17/16 Pct Recovery = 39% Analysis Date = 07/17/16 Pct Recovery = 39% Analysis Date = 07/12/16 Pct Recovery = 40% Analysis Date = 07/12/16 Pct Recovery = 40% Analysis Date = 07/07/16 Pct Recovery = 40% Analysis Date = 07/07/16 Pct Recovery = 40% Analysis Date = 07/02/16 Pct Recovery = 40% Analysis Date = 07/02/16 Pct Recovery = 40% Analysis Date = 06/27/16 Pct Recovery = 40% Analysis Date = 06/27/16 Pct Recovery = 40% Analysis Date = 06/22/16 Pct Recovery = 41% Analysis Date = 06/22/16 Pct Recovery = 41% Analysis Date = 06/17/16 Pct Recovery = 41% Analysis Date = 06/17/16 Pct Recovery = 41% Analysis Date = 06/12/16 Pct Recovery = 41% Analysis Date = 06/12/16 Pct Recovery = 41% Analysis Date = 06/07/16 Pct Recovery = 41% Analysis Date = 06/07/16 Pct Recovery = 41% Analysis Date = 06/02/16 Pct Recovery = 41% Analysis Date = 06/02/16 Pct Recovery = 41% Analysis Date = 05/28/16 Pct Recovery = 42% Analysis Date = 05/28/16 Pct Recovery = 42% Analysis Date = 05/23/16 Pct Recovery = 42% Analysis Date = 05/23/16 Pct Recovery = 42% Analysis Date = 05/18/16 Pct Recovery = 42% Analysis Date = 05/18/16 Pct Recovery = 42% Analysis Date = 05/13/16 Pct Recovery = 42% Analysis Date = 05/13/16 Pct Recovery = 42% Analysis Date = 05/08/16 Pct Recovery = 43% Analysis Date = 05/08/16 Pct Recovery = 43% Analysis Date = 05/03/16 Pct Recovery = 43% Analysis Date = 05/03/16 Pct Recovery = 43% Analysis Date = 04/28/16 Pct Recovery = 43% Analysis Date = 04/28/16 Pct Recovery = 43% Analysis Date = 04/23/16 Pct Recovery = 43% Analysis Date = 04/23/16 Pct Recovery = 43% Analysis Date = 04/18/16 Pct Recovery = 43% Analysis Date = 04/18/16 Pct Recovery = 43% Analysis Date = 04/13/16 Pct Recovery = 43% Analysis Date = 04/13/16 Pct Recovery = 43% Analysis Date = 04/08/16 Pct Recovery = 43% Analysis Date = 04/08/16 Pct Recovery = 43% Analysis Date = 04/03/16 Pct Recovery = 43% Analysis Date = 04/03/16 Pct Recovery = 43% Analysis Date = 03/29/16 Pct Recovery = 43% Analysis Date = 03/29/16 Pct Recovery = 43% Analysis Date = 03/24/16 Pct Recovery = 43% Analysis Date = 03/24/16 Pct Recovery = 43% Analysis Date = 03/19/16 Pct Recovery = 43% Analysis Date = 03/19/16 Pct Recovery = 43% Analysis Date = 03/14/16 Pct Recovery = 43% Analysis Date = 03/14/16 Pct Recovery = 43% Analysis Date = 03/09/16 Pct Recovery = 43% Analysis Date = 03/09/16 Pct Recovery = 43% Analysis Date = 03/04/16 Pct Recovery = 43% Analysis Date = 03/04/16 Pct Recovery = 43% Analysis Date = 02/28/16 Pct Recovery = 43% Analysis Date = 02/28/16 Pct Recovery = 43% Analysis Date = 02/23/16 Pct Recovery = 43% Analysis Date = 02/23/16 Pct Recovery = 43% Analysis Date = 02/18/16 Pct Recovery = 43% Analysis Date = 02/18/16 Pct Recovery = 43% Analysis Date = 02/13/16 Pct Recovery = 43% Analysis Date = 02/13/16 Pct Recovery = 43% Analysis Date = 02/08/16 Pct Recovery = 43% Analysis Date = 02/08/16 Pct Recovery = 43% Analysis Date = 02/03/16 Pct Recovery = 43% Analysis Date = 02/03/16 Pct Recovery = 43% Analysis Date = 01/29/16 Pct Recovery = 43% Analysis Date = 01/29/16 Pct Recovery = 43% Analysis Date = 01/24/16 Pct Recovery = 43% Analysis Date = 01/24/16 Pct Recovery = 43% Analysis Date = 01/19/16 Pct Recovery = 43% Analysis Date = 01/19/16 Pct Recovery = 43% Analysis Date = 01/14/16 Pct Recovery = 43% Analysis Date = 01/14/16 Pct Recovery = 43% Analysis Date = 01/09/16 Pct Recovery = 43% Analysis Date = 01/09/16 Pct Recovery = 43% Analysis Date = 01/04/16 Pct Recovery = 42% Analysis Date = 01/04/16 Pct Recovery = 42% Analysis Date = 12/30/15 Pct Recovery = 42% Analysis Date = 12/30/15 Pct Recovery = 42% Analysis Date = 12/25/15 Pct Recovery = 42% Analysis Date = 12/25/15 Pct Recovery = 42% Analysis Date = 12/20/15 Pct Recovery = 42% Analysis Date = 12/20/15 Pct Recovery = 42% Analysis Date = 12/15/15 Pct Recovery = 42% Analysis Date = 12/15/15 Pct Recovery = 42% Analysis Date = 12/10/15 Pct Recovery = 42% Analysis Date = 12/10/15 Pct Recovery = 42% Analysis Date = 12/05/15 Pct Recovery = 42% Analysis Date = 12/05/15 Pct Recovery = 42% Analysis Date = 11/30/15 Pct Recovery = 42% Analysis Date = 11/30/15 Pct Recovery = 42% Analysis Date = 11/25/15 Pct Recovery = 42% Analysis Date = 11/25/15 Pct Recovery = 42% Analysis Date = 11/20/15 Pct Recovery = 41% Analysis Date = 11/20/15 Pct Recovery = 41% Analysis Date = 11/15/15 Pct Recovery = 41% Analysis Date = 11/15/15 Pct Recovery = 41% Analysis Date = 11/10/15 Pct Recovery = 41% Analysis Date = 11/10/15 Pct Recovery = 41% Analysis Date = 11/05/15 Pct Recovery = 41% Analysis Date = 11/05/15 Pct Recovery = 41% Analysis Date = 10/31/15 Pct Recovery = 40% Analysis Date = 10/31/15 Pct Recovery = 40% Analysis Date = 10/26/15 Pct Recovery = 40% Analysis Date = 10/26/15 Pct Recovery = 40% Analysis Date = 10/21/15 Pct Recovery = 40% Analysis Date = 10/21/15 Pct Recovery = 40% Analysis Date = 10/16/15 Pct Recovery = 40% Analysis Date = 10/16/15 Pct Recovery = 40% Analysis Date = 10/11/15 Pct Recovery = 40% Analysis Date = 10/11/15 Pct Recovery = 40% Analysis Date = 10/06/15 Pct Recovery = 39% Analysis Date = 10/06/15 Pct Recovery = 39% Analysis Date = 10/01/15 Pct Recovery = 39% Analysis Date = 10/01/15 Pct Recovery = 39% Analysis Date = 09/26/15 Pct Recovery = 39% Analysis Date = 09/26/15 Pct Recovery = 39% Analysis Date = 09/21/15 Pct Recovery = 39% Analysis Date = 09/21/15 Pct Recovery = 39% Analysis Date = 09/16/15 Pct Recovery = 39% Analysis Date = 09/16/15 Pct Recovery = 39% Analysis Date = 09/11/15 Pct Recovery = 38% Analysis Date = 09/11/15 Pct Recovery = 38% Analysis Date = 09/05/15 Pct Recovery = 38% Analysis Date = 09/05/15 Pct Recovery = 38% Analysis Date = 08/31/15 Pct Recovery = 38% Analysis Date = 08/31/15 Pct Recovery = 38% Analysis Date = 08/26/15 Pct Recovery = 38% Analysis Date = 08/26/15 Pct Recovery = 38% Analysis Date = 08/21/15 Pct Recovery = 38% Analysis Date = 08/21/15 Pct Recovery = 38% Analysis Date = 08/16/15 Pct Recovery = 37% Analysis Date = 08/16/15 Pct Recovery = 37% Analysis Date = 08/11/15 Pct Recovery = 37% Analysis Date = 08/11/15 Pct Recovery = 37% Analysis Date = 08/06/15 Pct Recovery = 37% Analysis Date = 08/06/15 Pct Recovery = 37% Analysis Date = 08/01/15 Pct Recovery = 37% Analysis Date = 08/01/15 Pct Recovery = 37% Analysis Date = 07/27/15 Pct Recovery = 37% Analysis Date = 07/27/15 Pct Recovery = 37% Analysis Date = 07/22/15 Pct Recovery = 36% Analysis Date = 07/22/15 Pct Recovery = 36% Analysis Date = 07/17/15 Pct Recovery = 36% Analysis Date = 07/17/15 Pct Recovery = 36% Analysis Date = 07/12/15 Pct Recovery = 36% Analysis Date = 07/12/15 Pct Recovery = 36% Analysis Date = 07/07/15 Pct Recovery = 36% Analysis Date = 07/07/15 Pct Recovery = 36% Analysis Date = 07/02/15 Pct Recovery = 36% Analysis Date = 07/02/15 Pct Recovery = 36% Analysis Date = 06/27/15 Pct Recovery = 35% Analysis Date = 06/27/15 Pct Recovery = 35% Analysis Date = 06/22/15 Pct Recovery = 35% Analysis Date = 06/22/15 Pct Recovery = 35% Analysis Date = 06/17/15 Pct Recovery = 35% Analysis Date = 06/17/15 Pct Recovery = 35% Analysis Date = 06/12/15 Pct Recovery = 35% Analysis Date = 06/12/15 Pct Recovery = 35% Analysis Date = 06/07/15 Pct Recovery = 35% Analysis Date = 06/07/15 Pct Recovery = 35% Analysis Date = 06/02/15 Pct Recovery = 34% Analysis Date = 06/02/15 Pct Recovery = 34% Analysis Date = 05/28/15 Pct Recovery = 34% Analysis Date = 05/28/15 Pct Recovery = 34% Analysis Date = 05/23/15 Pct Recovery = 34% Analysis Date = 05/23/15 Pct Recovery = 34% Analysis Date = 05/18/15 Pct Recovery = 34% Analysis Date = 05/18/15 Pct Recovery = 34% Analysis Date = 05/13/15 Pct Recovery = 34% Analysis Date = 05/13/15 Pct Recovery = 34% Analysis Date = 05/08/15 Pct Recovery = 33% Analysis Date = 05/08/15 Pct Recovery = 33% Analysis Date = 05/03/15 Pct Recovery = 33% Analysis Date = 05/03/15 Pct Recovery = 33% Analysis Date = 04/28/15 Pct Recovery = 33% Analysis Date = 04/28/15 Pct Recovery = 33% Analysis Date = 04/23/15 Pct Recovery = 33% Analysis Date = 04/23/15 Pct Recovery = 33% Analysis Date = 04/18/15 Pct Recovery = 33% Analysis Date = 04/18/15 Pct Recovery = 33% Analysis Date = 04/13/15 Pct Recovery = 33% Analysis Date = 04/13/15 Pct Recovery = 33% Analysis Date = 04/08/15 Pct Recovery = 33% Analysis Date = 04/08/15 Pct Recovery = 33% Analysis Date = 04/03/15 Pct Recovery = 33% Analysis Date = 04/03/15 Pct Recovery = 33% Analysis Date = 03/29/15 Pct Recovery = 34% Analysis Date = 03/29/15 Pct Recovery = 34% Analysis Date = 03/24/15 Pct Recovery = 34% Analysis Date = 03/24/15 Pct Recovery = 34% Analysis Date = 03/19/15 Pct Recovery = 34% Analysis Date = 03/19/15 Pct Recovery = 34% Analysis Date = 03/14/15 Pct Recovery = 34% Analysis Date = 03/14/15 Pct Recovery = 34% Analysis Date = 03/09/15 Pct Recovery = 34% Analysis Date = 03/09/15 Pct Recovery = 34% Analysis Date = 03/04/15 Pct Recovery = 34% Analysis Date = 03/04/15 Pct Recovery = 34% Analysis Date = 02/27/15 Pct Recovery = 34% Analysis Date = 02/27/15 Pct Recovery = 34% Analysis Date = 02/22/15 Pct Recovery = 34% Analysis Date = 02/22/15 Pct Recovery = 34% Analysis Date = 02/17/15 Pct Recovery = 34% Analysis Date = 02/17/15 Pct Recovery = 34% Analysis Date = 02/12/15 Pct Recovery = 34% Analysis Date = 02/12/15 Pct Recovery = 34% Analysis Date = 02/07/15 Pct Recovery = 34% Analysis Date = 02/07/15 Pct Recovery = 34% Analysis Date = 02/02/15 Pct Recovery = 35% Analysis Date = 02/02/15 Pct Recovery = 35% Analysis Date = 01/28/15 Pct Recovery = 35% Analysis Date = 01/28/15 Pct Recovery = 35% Analysis Date = 01/23/15 Pct Recovery = 35% Analysis Date = 01/23/15 Pct Recovery = 35% Analysis Date = 01/18/15 Pct Recovery = 35% Analysis Date = 01/18/15 Pct Recovery = 35% Analysis Date = 01/13/15 Pct Recovery = 35% Analysis Date = 01/13/15 Pct Recovery = 35% Analysis Date = 01/08/15 Pct Recovery = 35% Analysis Date = 01/08/15 Pct Recovery = 35% Analysis Date = 01/03/15 Pct Recovery = 35% Analysis Date = 01/03/15 Pct Recovery = 35% Analysis Date = 12/29/14 Pct Recovery = 35% Analysis Date = 12/29/14 Pct Recovery = 35% Analysis Date = 12/24/14 Pct Recovery = 36% Analysis Date = 12/24/14 Pct Recovery = 36% Analysis Date = 12/19/14 Pct Recovery = 36% Analysis Date = 12/19/14 Pct Recovery = 36% Analysis Date = 12/14/14 Pct Recovery = 36% Analysis Date = 12/14/14 Pct Recovery = 36% Analysis Date = 12/09/14 Pct Recovery = 36% Analysis Date = 12/09/14 Pct Recovery = 36% Analysis Date = 12/04/14 Pct Recovery = 36% Analysis Date = 12/04/14 Pct Recovery = 36% Analysis Date = 11/29/14 Pct Recovery = 36% Analysis Date = 11/29/14 Pct Recovery = 36% Analysis Date = 11/24/14 Pct Recovery = 36% Analysis Date = 11/24/14 Pct Recovery = 36% Analysis Date = 11/19/14 Pct Recovery = 37% Analysis Date = 11/19/14 Pct Recovery = 37% Analysis Date = 11/14/14 Pct Recovery = 37% Analysis Date = 11/14/14 Pct Recovery = 37% Analysis Date = 11/09/14 Pct Recovery = 37% Analysis Date = 11/09/14 Pct Recovery = 37% Analysis Date = 11/04/14 Pct Recovery = 37% Analysis Date = 11/04/14 Pct Recovery = 37% Analysis Date = 10/30/14 Pct Recovery = 37% Analysis Date = 10/30/14 Pct Recovery = 37% Analysis Date = 10/25/14 Pct Recovery = 37% Analysis Date = 10/25/14 Pct Recovery = 37% Analysis Date = 10/20/14 Pct Recovery = 37% Analysis Date = 10/20/14 Pct Recovery = 37% Analysis Date = 10/15/14 Pct Recovery = 38% Analysis Date = 10/15/14 Pct Recovery = 38% Analysis Date = 10/10/14 Pct Recovery = 38% Analysis Date = 10/10/14 Pct Recovery = 38% Analysis Date = 10/05/14 Pct Recovery = 38% Analysis Date = 10/05/14 Pct Recovery = 38% Analysis Date = 09/30/14 Pct Recovery = 38% Analysis Date = 09/30/14 Pct Recovery = 38% Analysis Date = 09/25/14 Pct Recovery = 38% Analysis Date = 09/25/14 Pct Recovery = 38% Analysis Date = 09/20/14 Pct Recovery = 38% Analysis Date = 09/20/14 Pct Recovery = 38% Analysis Date = 09/15/14 Pct Recovery = 39% Analysis Date = 09/15/14 Pct Recovery = 39% Analysis Date = 09/10/14 Pct Recovery = 39% Analysis Date = 09/10/14 Pct Recovery = 39% Analysis Date = 09/05/14 Pct Recovery = 39% Analysis Date = 09/05/14 Pct Recovery = 39% Analysis Date = 08/31/14 Pct Recovery = 39% Analysis Date = 08/31/14 Pct Recovery = 39% Analysis Date = 08/26/14 Pct Recovery = 39% Analysis Date = 08/26/14 Pct Recovery = 39% Analysis Date = 08/21/14 Pct Recovery = 39% Analysis Date = 08/21/14 Pct Recovery = 39% Analysis Date = 08/16/14 Pct Recovery = 40% Analysis Date = 08/16/14 Pct Recovery = 40% Analysis Date = 08/11/14 Pct Recovery = 40% Analysis Date = 08/11/14 Pct Recovery = 40% Analysis Date = 08/06/14 Pct Recovery = 40% Analysis Date = 08/06/14 Pct Recovery = 40% Analysis Date = 08/01/14 Pct Recovery = 40% Analysis Date = 08/01/14 Pct Recovery = 40% Analysis Date = 07/27/14 Pct Recovery = 40% Analysis Date = 07/27/14 Pct Recovery = 40% Analysis Date = 07/22/14 Pct Recovery = 40% Analysis Date = 07/22/14 Pct Recovery = 40% Analysis Date = 07/17/14 Pct Recovery = 41% Analysis Date = 07/17/14 Pct Recovery = 41% Analysis Date = 07/12/14 Pct Recovery = 41% Analysis Date = 07/12/14 Pct Recovery = 41% Analysis Date = 07/07/14 Pct Recovery = 41% Analysis Date = 07/07/14 Pct Recovery = 41% Analysis Date = 07/02/14 Pct Recovery = 41% Analysis Date = 07/02/14 Pct Recovery = 41% Analysis Date = 06/27/14 Pct Recovery = 41% Analysis Date = 06/27/14 Pct Recovery = 41% Analysis Date = 06/22/14 Pct Recovery = 41% Analysis Date = 06/22/14 Pct Recovery = 41% Analysis Date = 06/17/14 Pct Recovery = 42% Analysis Date = 06/17/14 Pct Recovery = 42% Analysis Date = 06/12/14 Pct Recovery = 42% Analysis Date = 06/12/14 Pct Recovery = 42% Analysis Date = 06/07/14 Pct Recovery = 42% Analysis Date = 06/07/14 Pct Recovery = 42% Analysis Date = 06/02/14 Pct Recovery = 42% Analysis Date = 06/02/14 Pct Recovery = 42% Analysis Date = 05/28/14 Pct Recovery = 42% Analysis Date = 05/28/14 Pct Recovery = 42% Analysis Date = 05/23/14 Pct Recovery = 42% Analysis Date = 05/23/14 Pct Recovery = 42% Analysis Date = 05/18/14 Pct Recovery = 43% Analysis Date = 05/18/14 Pct Recovery = 43% Analysis Date = 05/13/14 Pct Recovery = 43% Analysis Date = 05/13/14 Pct Recovery = 43% Analysis Date = 05/08/14 Pct Recovery = 43% Analysis Date = 05/08/14 Pct Recovery = 43% Analysis Date = 05/03/14 Pct Recovery = 43% Analysis Date = 05/03/14 Pct Recovery = 43% Analysis Date = 04/28/14 Pct Recovery = 43% Analysis Date = 04/28/14 Pct Recovery = 43% Analysis Date = 04/23/14 Pct Recovery = 44% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
NORVERAPAMIL

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 1 13% . 13% 0%
>= Reporting Level 53 39% 19% 36% 13%
Total 54 38% 19% 35% 13%

Sample Statistics
NORVERAPAMIL

Characteristic N % % Basis
Plotted 54 82% Spiked
Estimated Values 54 82% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 2 3% Spiked
Spiked 66 .  
False Negatives 10 15% 10 out of 66
Not Spiked 49 .  
False Positives 0 0% 0 out of 49

BQS OBSP Determination:
OMEPRAZOLE + ESOMEPRAZOLE
METHOD: 2440 , TESTIDCODE: 67512LCM56
Open Data Set

Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 42% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 37% Analysis Date = 11/24/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 24% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 80 µl & Abs 051315: 80 µl Pct Recovery = 36% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 80 µl & ERA 0406-15-08: 80 µl Pct Recovery = 48% Analysis Date = 11/05/15 SpikeMix = ERA 0406-15-08: 80 µl & Abs 052215: 80 µl Pct Recovery = 13% Analysis Date = 11/18/16 SpikeMix = ERA 04281604: 80 µl & ERA 04281603: 80 µl Pct Recovery = 38% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & ERA 04281604: 80 µl Pct Recovery = 40% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 28% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 33% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 33% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 29% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 11% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 20% Analysis Date = 12/06/14 SpikeMix = ERA 0318-14-02: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 8% Analysis Date = 07/26/14 SpikeMix = ERA 0319-14-05: 60 µl & ERA 0318-14-02: 60 µl Pct Recovery = 6% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 34% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 32% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-07A: 40 µl & Abs 051315: 40 µl Pct Recovery = 31% Analysis Date = 07/30/15 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 26% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 85% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 30% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 27% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 27% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 23% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 26% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 20% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 27% Analysis Date = 12/07/14 SpikeMix = ERA 0318-14-02: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 15% Analysis Date = 06/26/15 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 27% Analysis Date = 04/27/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 55% Analysis Date = 11/25/15 SpikeMix = Abs 050115: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 28% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 28% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 27% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 31% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 30% Analysis Date = 01/19/17 Pct Recovery = 40% Analysis Date = 01/14/17 Pct Recovery = 39% Analysis Date = 01/14/17 Pct Recovery = 39% Analysis Date = 01/09/17 Pct Recovery = 39% Analysis Date = 01/09/17 Pct Recovery = 39% Analysis Date = 01/05/17 Pct Recovery = 38% Analysis Date = 01/05/17 Pct Recovery = 38% Analysis Date = 12/31/16 Pct Recovery = 38% Analysis Date = 12/31/16 Pct Recovery = 38% Analysis Date = 12/27/16 Pct Recovery = 37% Analysis Date = 12/27/16 Pct Recovery = 37% Analysis Date = 12/22/16 Pct Recovery = 37% Analysis Date = 12/22/16 Pct Recovery = 37% Analysis Date = 12/18/16 Pct Recovery = 36% Analysis Date = 12/18/16 Pct Recovery = 36% Analysis Date = 12/13/16 Pct Recovery = 36% Analysis Date = 12/13/16 Pct Recovery = 36% Analysis Date = 12/09/16 Pct Recovery = 35% Analysis Date = 12/09/16 Pct Recovery = 35% Analysis Date = 12/04/16 Pct Recovery = 35% Analysis Date = 12/04/16 Pct Recovery = 35% Analysis Date = 11/30/16 Pct Recovery = 34% Analysis Date = 11/30/16 Pct Recovery = 34% Analysis Date = 11/25/16 Pct Recovery = 34% Analysis Date = 11/25/16 Pct Recovery = 34% Analysis Date = 11/20/16 Pct Recovery = 33% Analysis Date = 11/20/16 Pct Recovery = 33% Analysis Date = 11/16/16 Pct Recovery = 33% Analysis Date = 11/16/16 Pct Recovery = 33% Analysis Date = 11/11/16 Pct Recovery = 33% Analysis Date = 11/11/16 Pct Recovery = 33% Analysis Date = 11/07/16 Pct Recovery = 32% Analysis Date = 11/07/16 Pct Recovery = 32% Analysis Date = 11/02/16 Pct Recovery = 32% Analysis Date = 11/02/16 Pct Recovery = 32% Analysis Date = 10/29/16 Pct Recovery = 31% Analysis Date = 10/29/16 Pct Recovery = 31% Analysis Date = 10/24/16 Pct Recovery = 31% Analysis Date = 10/24/16 Pct Recovery = 31% Analysis Date = 10/20/16 Pct Recovery = 30% Analysis Date = 10/20/16 Pct Recovery = 30% Analysis Date = 10/15/16 Pct Recovery = 30% Analysis Date = 10/15/16 Pct Recovery = 30% Analysis Date = 10/11/16 Pct Recovery = 29% Analysis Date = 10/11/16 Pct Recovery = 29% Analysis Date = 10/06/16 Pct Recovery = 29% Analysis Date = 10/06/16 Pct Recovery = 29% Analysis Date = 10/02/16 Pct Recovery = 28% Analysis Date = 10/02/16 Pct Recovery = 28% Analysis Date = 09/27/16 Pct Recovery = 28% Analysis Date = 09/27/16 Pct Recovery = 28% Analysis Date = 09/22/16 Pct Recovery = 27% Analysis Date = 09/22/16 Pct Recovery = 27% Analysis Date = 09/18/16 Pct Recovery = 27% Analysis Date = 09/18/16 Pct Recovery = 27% Analysis Date = 09/13/16 Pct Recovery = 26% Analysis Date = 09/13/16 Pct Recovery = 26% Analysis Date = 09/09/16 Pct Recovery = 26% Analysis Date = 09/09/16 Pct Recovery = 26% Analysis Date = 09/04/16 Pct Recovery = 25% Analysis Date = 09/04/16 Pct Recovery = 25% Analysis Date = 08/31/16 Pct Recovery = 25% Analysis Date = 08/31/16 Pct Recovery = 25% Analysis Date = 08/26/16 Pct Recovery = 24% Analysis Date = 08/26/16 Pct Recovery = 24% Analysis Date = 08/22/16 Pct Recovery = 24% Analysis Date = 08/22/16 Pct Recovery = 24% Analysis Date = 08/17/16 Pct Recovery = 23% Analysis Date = 08/17/16 Pct Recovery = 23% Analysis Date = 08/13/16 Pct Recovery = 22% Analysis Date = 08/13/16 Pct Recovery = 22% Analysis Date = 08/08/16 Pct Recovery = 23% Analysis Date = 08/08/16 Pct Recovery = 23% Analysis Date = 08/04/16 Pct Recovery = 23% Analysis Date = 08/04/16 Pct Recovery = 23% Analysis Date = 07/30/16 Pct Recovery = 24% Analysis Date = 07/30/16 Pct Recovery = 24% Analysis Date = 07/25/16 Pct Recovery = 25% Analysis Date = 07/25/16 Pct Recovery = 25% Analysis Date = 07/21/16 Pct Recovery = 26% Analysis Date = 07/21/16 Pct Recovery = 26% Analysis Date = 07/16/16 Pct Recovery = 27% Analysis Date = 07/16/16 Pct Recovery = 27% Analysis Date = 07/12/16 Pct Recovery = 28% Analysis Date = 07/12/16 Pct Recovery = 28% Analysis Date = 07/07/16 Pct Recovery = 28% Analysis Date = 07/07/16 Pct Recovery = 28% Analysis Date = 07/03/16 Pct Recovery = 29% Analysis Date = 07/03/16 Pct Recovery = 29% Analysis Date = 06/28/16 Pct Recovery = 30% Analysis Date = 06/28/16 Pct Recovery = 30% Analysis Date = 06/24/16 Pct Recovery = 31% Analysis Date = 06/24/16 Pct Recovery = 31% Analysis Date = 06/19/16 Pct Recovery = 32% Analysis Date = 06/19/16 Pct Recovery = 32% Analysis Date = 06/15/16 Pct Recovery = 33% Analysis Date = 06/15/16 Pct Recovery = 33% Analysis Date = 06/10/16 Pct Recovery = 33% Analysis Date = 06/10/16 Pct Recovery = 33% Analysis Date = 06/06/16 Pct Recovery = 34% Analysis Date = 06/06/16 Pct Recovery = 34% Analysis Date = 06/01/16 Pct Recovery = 35% Analysis Date = 06/01/16 Pct Recovery = 35% Analysis Date = 05/27/16 Pct Recovery = 36% Analysis Date = 05/27/16 Pct Recovery = 36% Analysis Date = 05/23/16 Pct Recovery = 37% Analysis Date = 05/23/16 Pct Recovery = 37% Analysis Date = 05/18/16 Pct Recovery = 38% Analysis Date = 05/18/16 Pct Recovery = 38% Analysis Date = 05/14/16 Pct Recovery = 39% Analysis Date = 05/14/16 Pct Recovery = 39% Analysis Date = 05/09/16 Pct Recovery = 39% Analysis Date = 05/09/16 Pct Recovery = 39% Analysis Date = 05/05/16 Pct Recovery = 40% Analysis Date = 05/05/16 Pct Recovery = 40% Analysis Date = 04/30/16 Pct Recovery = 41% Analysis Date = 04/30/16 Pct Recovery = 41% Analysis Date = 04/26/16 Pct Recovery = 42% Analysis Date = 04/26/16 Pct Recovery = 42% Analysis Date = 04/21/16 Pct Recovery = 41% Analysis Date = 04/21/16 Pct Recovery = 41% Analysis Date = 04/17/16 Pct Recovery = 41% Analysis Date = 04/17/16 Pct Recovery = 41% Analysis Date = 04/12/16 Pct Recovery = 41% Analysis Date = 04/12/16 Pct Recovery = 41% Analysis Date = 04/07/16 Pct Recovery = 41% Analysis Date = 04/07/16 Pct Recovery = 41% Analysis Date = 04/03/16 Pct Recovery = 41% Analysis Date = 04/03/16 Pct Recovery = 41% Analysis Date = 03/29/16 Pct Recovery = 40% Analysis Date = 03/29/16 Pct Recovery = 40% Analysis Date = 03/25/16 Pct Recovery = 40% Analysis Date = 03/25/16 Pct Recovery = 40% Analysis Date = 03/20/16 Pct Recovery = 40% Analysis Date = 03/20/16 Pct Recovery = 40% Analysis Date = 03/16/16 Pct Recovery = 40% Analysis Date = 03/16/16 Pct Recovery = 40% Analysis Date = 03/11/16 Pct Recovery = 39% Analysis Date = 03/11/16 Pct Recovery = 39% Analysis Date = 03/07/16 Pct Recovery = 39% Analysis Date = 03/07/16 Pct Recovery = 39% Analysis Date = 03/02/16 Pct Recovery = 39% Analysis Date = 03/02/16 Pct Recovery = 39% Analysis Date = 02/27/16 Pct Recovery = 39% Analysis Date = 02/27/16 Pct Recovery = 39% Analysis Date = 02/22/16 Pct Recovery = 39% Analysis Date = 02/22/16 Pct Recovery = 39% Analysis Date = 02/18/16 Pct Recovery = 38% Analysis Date = 02/18/16 Pct Recovery = 38% Analysis Date = 02/13/16 Pct Recovery = 38% Analysis Date = 02/13/16 Pct Recovery = 38% Analysis Date = 02/08/16 Pct Recovery = 38% Analysis Date = 02/08/16 Pct Recovery = 38% Analysis Date = 02/04/16 Pct Recovery = 38% Analysis Date = 02/04/16 Pct Recovery = 38% Analysis Date = 01/30/16 Pct Recovery = 37% Analysis Date = 01/30/16 Pct Recovery = 37% Analysis Date = 01/26/16 Pct Recovery = 37% Analysis Date = 01/26/16 Pct Recovery = 37% Analysis Date = 01/21/16 Pct Recovery = 37% Analysis Date = 01/21/16 Pct Recovery = 37% Analysis Date = 01/17/16 Pct Recovery = 37% Analysis Date = 01/17/16 Pct Recovery = 37% Analysis Date = 01/12/16 Pct Recovery = 36% Analysis Date = 01/12/16 Pct Recovery = 36% Analysis Date = 01/08/16 Pct Recovery = 36% Analysis Date = 01/08/16 Pct Recovery = 36% Analysis Date = 01/03/16 Pct Recovery = 36% Analysis Date = 01/03/16 Pct Recovery = 36% Analysis Date = 12/30/15 Pct Recovery = 36% Analysis Date = 12/30/15 Pct Recovery = 36% Analysis Date = 12/25/15 Pct Recovery = 35% Analysis Date = 12/25/15 Pct Recovery = 35% Analysis Date = 12/21/15 Pct Recovery = 35% Analysis Date = 12/21/15 Pct Recovery = 35% Analysis Date = 12/16/15 Pct Recovery = 35% Analysis Date = 12/16/15 Pct Recovery = 35% Analysis Date = 12/11/15 Pct Recovery = 35% Analysis Date = 12/11/15 Pct Recovery = 35% Analysis Date = 12/07/15 Pct Recovery = 34% Analysis Date = 12/07/15 Pct Recovery = 34% Analysis Date = 12/02/15 Pct Recovery = 34% Analysis Date = 12/02/15 Pct Recovery = 34% Analysis Date = 11/28/15 Pct Recovery = 34% Analysis Date = 11/28/15 Pct Recovery = 34% Analysis Date = 11/23/15 Pct Recovery = 33% Analysis Date = 11/23/15 Pct Recovery = 33% Analysis Date = 11/19/15 Pct Recovery = 33% Analysis Date = 11/19/15 Pct Recovery = 33% Analysis Date = 11/14/15 Pct Recovery = 33% Analysis Date = 11/14/15 Pct Recovery = 33% Analysis Date = 11/10/15 Pct Recovery = 33% Analysis Date = 11/10/15 Pct Recovery = 33% Analysis Date = 11/05/15 Pct Recovery = 32% Analysis Date = 11/05/15 Pct Recovery = 32% Analysis Date = 11/01/15 Pct Recovery = 32% Analysis Date = 11/01/15 Pct Recovery = 32% Analysis Date = 10/27/15 Pct Recovery = 32% Analysis Date = 10/27/15 Pct Recovery = 32% Analysis Date = 10/23/15 Pct Recovery = 31% Analysis Date = 10/23/15 Pct Recovery = 31% Analysis Date = 10/18/15 Pct Recovery = 31% Analysis Date = 10/18/15 Pct Recovery = 31% Analysis Date = 10/13/15 Pct Recovery = 31% Analysis Date = 10/13/15 Pct Recovery = 31% Analysis Date = 10/09/15 Pct Recovery = 30% Analysis Date = 10/09/15 Pct Recovery = 30% Analysis Date = 10/04/15 Pct Recovery = 30% Analysis Date = 10/04/15 Pct Recovery = 30% Analysis Date = 09/30/15 Pct Recovery = 30% Analysis Date = 09/30/15 Pct Recovery = 30% Analysis Date = 09/25/15 Pct Recovery = 29% Analysis Date = 09/25/15 Pct Recovery = 29% Analysis Date = 09/21/15 Pct Recovery = 29% Analysis Date = 09/21/15 Pct Recovery = 29% Analysis Date = 09/16/15 Pct Recovery = 29% Analysis Date = 09/16/15 Pct Recovery = 29% Analysis Date = 09/12/15 Pct Recovery = 29% Analysis Date = 09/12/15 Pct Recovery = 29% Analysis Date = 09/07/15 Pct Recovery = 28% Analysis Date = 09/07/15 Pct Recovery = 28% Analysis Date = 09/03/15 Pct Recovery = 28% Analysis Date = 09/03/15 Pct Recovery = 28% Analysis Date = 08/29/15 Pct Recovery = 28% Analysis Date = 08/29/15 Pct Recovery = 28% Analysis Date = 08/24/15 Pct Recovery = 27% Analysis Date = 08/24/15 Pct Recovery = 27% Analysis Date = 08/20/15 Pct Recovery = 27% Analysis Date = 08/20/15 Pct Recovery = 27% Analysis Date = 08/15/15 Pct Recovery = 27% Analysis Date = 08/15/15 Pct Recovery = 27% Analysis Date = 08/11/15 Pct Recovery = 26% Analysis Date = 08/11/15 Pct Recovery = 26% Analysis Date = 08/06/15 Pct Recovery = 26% Analysis Date = 08/06/15 Pct Recovery = 26% Analysis Date = 08/02/15 Pct Recovery = 26% Analysis Date = 08/02/15 Pct Recovery = 26% Analysis Date = 07/28/15 Pct Recovery = 25% Analysis Date = 07/28/15 Pct Recovery = 25% Analysis Date = 07/24/15 Pct Recovery = 25% Analysis Date = 07/24/15 Pct Recovery = 25% Analysis Date = 07/19/15 Pct Recovery = 25% Analysis Date = 07/19/15 Pct Recovery = 25% Analysis Date = 07/15/15 Pct Recovery = 25% Analysis Date = 07/15/15 Pct Recovery = 25% Analysis Date = 07/10/15 Pct Recovery = 24% Analysis Date = 07/10/15 Pct Recovery = 24% Analysis Date = 07/06/15 Pct Recovery = 24% Analysis Date = 07/06/15 Pct Recovery = 24% Analysis Date = 07/01/15 Pct Recovery = 24% Analysis Date = 07/01/15 Pct Recovery = 24% Analysis Date = 06/26/15 Pct Recovery = 24% Analysis Date = 06/26/15 Pct Recovery = 24% Analysis Date = 06/22/15 Pct Recovery = 23% Analysis Date = 06/22/15 Pct Recovery = 23% Analysis Date = 06/17/15 Pct Recovery = 23% Analysis Date = 06/17/15 Pct Recovery = 23% Analysis Date = 06/13/15 Pct Recovery = 23% Analysis Date = 06/13/15 Pct Recovery = 23% Analysis Date = 06/08/15 Pct Recovery = 23% Analysis Date = 06/08/15 Pct Recovery = 23% Analysis Date = 06/04/15 Pct Recovery = 22% Analysis Date = 06/04/15 Pct Recovery = 22% Analysis Date = 05/30/15 Pct Recovery = 22% Analysis Date = 05/30/15 Pct Recovery = 22% Analysis Date = 05/26/15 Pct Recovery = 22% Analysis Date = 05/26/15 Pct Recovery = 22% Analysis Date = 05/21/15 Pct Recovery = 22% Analysis Date = 05/21/15 Pct Recovery = 22% Analysis Date = 05/17/15 Pct Recovery = 21% Analysis Date = 05/17/15 Pct Recovery = 21% Analysis Date = 05/12/15 Pct Recovery = 21% Analysis Date = 05/12/15 Pct Recovery = 21% Analysis Date = 05/08/15 Pct Recovery = 21% Analysis Date = 05/08/15 Pct Recovery = 21% Analysis Date = 05/03/15 Pct Recovery = 20% Analysis Date = 05/03/15 Pct Recovery = 20% Analysis Date = 04/28/15 Pct Recovery = 20% Analysis Date = 04/28/15 Pct Recovery = 20% Analysis Date = 04/24/15 Pct Recovery = 20% Analysis Date = 04/24/15 Pct Recovery = 20% Analysis Date = 04/19/15 Pct Recovery = 20% Analysis Date = 04/19/15 Pct Recovery = 20% Analysis Date = 04/15/15 Pct Recovery = 19% Analysis Date = 04/15/15 Pct Recovery = 19% Analysis Date = 04/10/15 Pct Recovery = 19% Analysis Date = 04/10/15 Pct Recovery = 19% Analysis Date = 04/06/15 Pct Recovery = 19% Analysis Date = 04/06/15 Pct Recovery = 19% Analysis Date = 04/01/15 Pct Recovery = 19% Analysis Date = 04/01/15 Pct Recovery = 19% Analysis Date = 03/28/15 Pct Recovery = 18% Analysis Date = 03/28/15 Pct Recovery = 18% Analysis Date = 03/23/15 Pct Recovery = 18% Analysis Date = 03/23/15 Pct Recovery = 18% Analysis Date = 03/19/15 Pct Recovery = 18% Analysis Date = 03/19/15 Pct Recovery = 18% Analysis Date = 03/14/15 Pct Recovery = 18% Analysis Date = 03/14/15 Pct Recovery = 18% Analysis Date = 03/10/15 Pct Recovery = 17% Analysis Date = 03/10/15 Pct Recovery = 17% Analysis Date = 03/05/15 Pct Recovery = 17% Analysis Date = 03/05/15 Pct Recovery = 17% Analysis Date = 02/28/15 Pct Recovery = 17% Analysis Date = 02/28/15 Pct Recovery = 17% Analysis Date = 02/24/15 Pct Recovery = 16% Analysis Date = 02/24/15 Pct Recovery = 16% Analysis Date = 02/19/15 Pct Recovery = 16% Analysis Date = 02/19/15 Pct Recovery = 16% Analysis Date = 02/15/15 Pct Recovery = 16% Analysis Date = 02/15/15 Pct Recovery = 16% Analysis Date = 02/10/15 Pct Recovery = 16% Analysis Date = 02/10/15 Pct Recovery = 16% Analysis Date = 02/06/15 Pct Recovery = 15% Analysis Date = 02/06/15 Pct Recovery = 15% Analysis Date = 02/01/15 Pct Recovery = 15% Analysis Date = 02/01/15 Pct Recovery = 15% Analysis Date = 01/28/15 Pct Recovery = 15% Analysis Date = 01/28/15 Pct Recovery = 15% Analysis Date = 01/23/15 Pct Recovery = 15% Analysis Date = 01/23/15 Pct Recovery = 15% Analysis Date = 01/19/15 Pct Recovery = 14% Analysis Date = 01/19/15 Pct Recovery = 14% Analysis Date = 01/14/15 Pct Recovery = 14% Analysis Date = 01/14/15 Pct Recovery = 14% Analysis Date = 01/09/15 Pct Recovery = 14% Analysis Date = 01/09/15 Pct Recovery = 14% Analysis Date = 01/05/15 Pct Recovery = 14% Analysis Date = 01/05/15 Pct Recovery = 14% Analysis Date = 12/31/14 Pct Recovery = 13% Analysis Date = 12/31/14 Pct Recovery = 13% Analysis Date = 12/27/14 Pct Recovery = 13% Analysis Date = 12/27/14 Pct Recovery = 13% Analysis Date = 12/22/14 Pct Recovery = 13% Analysis Date = 12/22/14 Pct Recovery = 13% Analysis Date = 12/18/14 Pct Recovery = 13% Analysis Date = 12/18/14 Pct Recovery = 13% Analysis Date = 12/13/14 Pct Recovery = 12% Analysis Date = 12/13/14 Pct Recovery = 12% Analysis Date = 12/09/14 Pct Recovery = 12% Analysis Date = 12/09/14 Pct Recovery = 12% Analysis Date = 12/04/14 Pct Recovery = 12% Analysis Date = 12/04/14 Pct Recovery = 12% Analysis Date = 11/30/14 Pct Recovery = 11% Analysis Date = 11/30/14 Pct Recovery = 11% Analysis Date = 11/25/14 Pct Recovery = 11% Analysis Date = 11/25/14 Pct Recovery = 11% Analysis Date = 11/21/14 Pct Recovery = 11% Analysis Date = 11/21/14 Pct Recovery = 11% Analysis Date = 11/16/14 Pct Recovery = 11% Analysis Date = 11/16/14 Pct Recovery = 11% Analysis Date = 11/11/14 Pct Recovery = 10% Analysis Date = 11/11/14 Pct Recovery = 10% Analysis Date = 11/07/14 Pct Recovery = 10% Analysis Date = 11/07/14 Pct Recovery = 10% Analysis Date = 11/02/14 Pct Recovery = 10% Analysis Date = 11/02/14 Pct Recovery = 10% Analysis Date = 10/29/14 Pct Recovery = 10% Analysis Date = 10/29/14 Pct Recovery = 10% Analysis Date = 10/24/14 Pct Recovery = 9% Analysis Date = 10/24/14 Pct Recovery = 9% Analysis Date = 10/20/14 Pct Recovery = 9% Analysis Date = 10/20/14 Pct Recovery = 9% Analysis Date = 10/15/14 Pct Recovery = 9% Analysis Date = 10/15/14 Pct Recovery = 9% Analysis Date = 10/11/14 Pct Recovery = 9% Analysis Date = 10/11/14 Pct Recovery = 9% Analysis Date = 10/06/14 Pct Recovery = 8% Analysis Date = 10/06/14 Pct Recovery = 8% Analysis Date = 10/02/14 Pct Recovery = 8% Analysis Date = 10/02/14 Pct Recovery = 8% Analysis Date = 09/27/14 Pct Recovery = 8% Analysis Date = 09/27/14 Pct Recovery = 8% Analysis Date = 09/23/14 Pct Recovery = 8% Analysis Date = 09/23/14 Pct Recovery = 8% Analysis Date = 09/18/14 Pct Recovery = 7% Analysis Date = 09/18/14 Pct Recovery = 7% Analysis Date = 09/13/14 Pct Recovery = 7% Analysis Date = 09/13/14 Pct Recovery = 7% Analysis Date = 09/09/14 Pct Recovery = 7% Analysis Date = 09/09/14 Pct Recovery = 7% Analysis Date = 09/04/14 Pct Recovery = 6% Analysis Date = 09/04/14 Pct Recovery = 6% Analysis Date = 08/31/14 Pct Recovery = 6% Analysis Date = 08/31/14 Pct Recovery = 6% Analysis Date = 08/26/14 Pct Recovery = 6% Analysis Date = 08/26/14 Pct Recovery = 6% Analysis Date = 08/22/14 Pct Recovery = 6% Analysis Date = 08/22/14 Pct Recovery = 6% Analysis Date = 08/17/14 Pct Recovery = 5% Analysis Date = 08/17/14 Pct Recovery = 5% Analysis Date = 08/13/14 Pct Recovery = 5% Analysis Date = 08/13/14 Pct Recovery = 5% Analysis Date = 08/08/14 Pct Recovery = 5% Analysis Date = 08/08/14 Pct Recovery = 5% Analysis Date = 08/04/14 Pct Recovery = 5% Analysis Date = 08/04/14 Pct Recovery = 5% Analysis Date = 07/30/14 Pct Recovery = 4% Analysis Date = 07/30/14 Pct Recovery = 4% Analysis Date = 07/26/14 Pct Recovery = 4% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
OMEPRAZOLE + ESOMEPRAZOLE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 4 29% 2% 29% 2%
>= Reporting Level 32 30% 15% 28% 8%
Total 36 30% 14% 28% 7%

Sample Statistics
OMEPRAZOLE + ESOMEPRAZOLE

Characteristic N % % Basis
Plotted 36 48% Spiked
Estimated Values 12 16% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 9 12% Spiked
Spiked 75 .  
False Negatives 30 40% 30 out of 75
Not Spiked 40 .  
False Positives 0 0% 0 out of 40

BQS OBSP Determination:
OSELTAMIVIR
METHOD: 2440 , TESTIDCODE: 67511LCM56
Open Data Set

Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 55% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 57% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 80 µl & ERA 0406-15-08: 80 µl Pct Recovery = 51% Analysis Date = 11/05/15 SpikeMix = ERA 0406-15-08: 80 µl & Abs 052215: 80 µl Pct Recovery = 58% Analysis Date = 11/24/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 48% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 80 µl & Abs 051315: 80 µl Pct Recovery = 51% Analysis Date = 10/01/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 24% Analysis Date = 11/18/16 SpikeMix = ERA 04281604: 80 µl & ERA 04281603: 80 µl Pct Recovery = 57% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & ERA 04281604: 80 µl Pct Recovery = 54% Analysis Date = 09/24/16 SpikeMix = Crescent EN160610015: 80 µl & Abs 061416: 80 µl Pct Recovery = 47% Analysis Date = 09/24/16 SpikeMix = Abs 061416: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 41% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 52% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 48% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 51% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 51% Analysis Date = 04/29/15 SpikeMix = ERA 0319-14-05: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 74% Analysis Date = 02/06/15 SpikeMix = Abs 041814: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 60% Analysis Date = 12/06/14 SpikeMix = ERA 0318-14-02: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 54% Analysis Date = 10/11/14 SpikeMix = ERA 0318-14-02: 60 µl & ERA 0319-14-04: 60 µl Pct Recovery = 42% Analysis Date = 08/21/14 SpikeMix = ERA 0318-14-02: 60 µl & Abs 041714: 60 µl Pct Recovery = 39% Analysis Date = 07/26/14 SpikeMix = ERA 0319-14-05: 60 µl & ERA 0318-14-02: 60 µl Pct Recovery = 55% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-08: 40 µl & Abs 052215: 40 µl Pct Recovery = 54% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 55% Analysis Date = 11/04/15 SpikeMix = ERA 0406-15-07A: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 52% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-08: 40 µl & ERA 0406-15-09: 40 µl Pct Recovery = 54% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 46% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 37% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-07A: 40 µl & Abs 051315: 40 µl Pct Recovery = 43% Analysis Date = 07/31/15 SpikeMix = Abs 051315: 40 µl & Abs 052215: 40 µl Pct Recovery = 42% Analysis Date = 07/30/15 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 53% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 80% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 86% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 62% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 63% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 54% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 56% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 43% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 40% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 39% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 39% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 35% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 40% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 40% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 37% Analysis Date = 12/07/14 SpikeMix = ERA 0318-14-02: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 64% Analysis Date = 11/04/14 SpikeMix = Abs 041814: 8 µl & ERA 0318-14-02: 8 µl Pct Recovery = 51% Analysis Date = 10/10/14 SpikeMix = Abs 041814: 30 µl & ERA 0318-14-02: 30 µl Pct Recovery = 41% Analysis Date = 08/30/14 SpikeMix = ERA 0318-14-02: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 49% Analysis Date = 07/20/14 SpikeMix = ERA 0318-14-02: 30 µl & Abs 041714: 30 µl Pct Recovery = 35% Analysis Date = 04/27/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 75% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 64% Analysis Date = 11/25/15 SpikeMix = Abs 050115: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 68% Analysis Date = 09/15/15 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 57% Analysis Date = 02/23/16 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 52% Analysis Date = 08/11/15 SpikeMix = Abs 050115: 20 µl & Abs 051315: 20 µl Pct Recovery = 34% Analysis Date = 06/26/15 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 53% Analysis Date = 06/09/15 SpikeMix = Abs 051315: 20 µl & Abs 050115: 20 µl Pct Recovery = 50% Analysis Date = 01/05/17 Pct Recovery = 58% Analysis Date = 12/31/16 Pct Recovery = 57% Analysis Date = 12/31/16 Pct Recovery = 57% Analysis Date = 12/27/16 Pct Recovery = 57% Analysis Date = 12/27/16 Pct Recovery = 57% Analysis Date = 12/22/16 Pct Recovery = 57% Analysis Date = 12/22/16 Pct Recovery = 57% Analysis Date = 12/18/16 Pct Recovery = 57% Analysis Date = 12/18/16 Pct Recovery = 57% Analysis Date = 12/13/16 Pct Recovery = 56% Analysis Date = 12/13/16 Pct Recovery = 56% Analysis Date = 12/09/16 Pct Recovery = 56% Analysis Date = 12/09/16 Pct Recovery = 56% Analysis Date = 12/04/16 Pct Recovery = 56% Analysis Date = 12/04/16 Pct Recovery = 56% Analysis Date = 11/30/16 Pct Recovery = 55% Analysis Date = 11/30/16 Pct Recovery = 55% Analysis Date = 11/25/16 Pct Recovery = 55% Analysis Date = 11/25/16 Pct Recovery = 55% Analysis Date = 11/21/16 Pct Recovery = 55% Analysis Date = 11/21/16 Pct Recovery = 55% Analysis Date = 11/16/16 Pct Recovery = 55% Analysis Date = 11/16/16 Pct Recovery = 55% Analysis Date = 11/12/16 Pct Recovery = 54% Analysis Date = 11/12/16 Pct Recovery = 54% Analysis Date = 11/07/16 Pct Recovery = 54% Analysis Date = 11/07/16 Pct Recovery = 54% Analysis Date = 11/03/16 Pct Recovery = 54% Analysis Date = 11/03/16 Pct Recovery = 54% Analysis Date = 10/29/16 Pct Recovery = 54% Analysis Date = 10/29/16 Pct Recovery = 54% Analysis Date = 10/25/16 Pct Recovery = 53% Analysis Date = 10/25/16 Pct Recovery = 53% Analysis Date = 10/20/16 Pct Recovery = 53% Analysis Date = 10/20/16 Pct Recovery = 53% Analysis Date = 10/16/16 Pct Recovery = 53% Analysis Date = 10/16/16 Pct Recovery = 53% Analysis Date = 10/11/16 Pct Recovery = 53% Analysis Date = 10/11/16 Pct Recovery = 53% Analysis Date = 10/07/16 Pct Recovery = 53% Analysis Date = 10/07/16 Pct Recovery = 53% Analysis Date = 10/02/16 Pct Recovery = 52% Analysis Date = 10/02/16 Pct Recovery = 52% Analysis Date = 09/28/16 Pct Recovery = 52% Analysis Date = 09/28/16 Pct Recovery = 52% Analysis Date = 09/23/16 Pct Recovery = 52% Analysis Date = 09/23/16 Pct Recovery = 52% Analysis Date = 09/19/16 Pct Recovery = 52% Analysis Date = 09/19/16 Pct Recovery = 52% Analysis Date = 09/14/16 Pct Recovery = 52% Analysis Date = 09/14/16 Pct Recovery = 52% Analysis Date = 09/10/16 Pct Recovery = 51% Analysis Date = 09/10/16 Pct Recovery = 51% Analysis Date = 09/05/16 Pct Recovery = 51% Analysis Date = 09/05/16 Pct Recovery = 51% Analysis Date = 09/01/16 Pct Recovery = 51% Analysis Date = 09/01/16 Pct Recovery = 51% Analysis Date = 08/27/16 Pct Recovery = 51% Analysis Date = 08/27/16 Pct Recovery = 51% Analysis Date = 08/23/16 Pct Recovery = 51% Analysis Date = 08/23/16 Pct Recovery = 51% Analysis Date = 08/18/16 Pct Recovery = 51% Analysis Date = 08/18/16 Pct Recovery = 51% Analysis Date = 08/14/16 Pct Recovery = 51% Analysis Date = 08/14/16 Pct Recovery = 51% Analysis Date = 08/09/16 Pct Recovery = 50% Analysis Date = 08/09/16 Pct Recovery = 50% Analysis Date = 08/05/16 Pct Recovery = 50% Analysis Date = 08/05/16 Pct Recovery = 50% Analysis Date = 07/31/16 Pct Recovery = 50% Analysis Date = 07/31/16 Pct Recovery = 50% Analysis Date = 07/27/16 Pct Recovery = 50% Analysis Date = 07/27/16 Pct Recovery = 50% Analysis Date = 07/22/16 Pct Recovery = 50% Analysis Date = 07/22/16 Pct Recovery = 50% Analysis Date = 07/18/16 Pct Recovery = 50% Analysis Date = 07/18/16 Pct Recovery = 50% Analysis Date = 07/13/16 Pct Recovery = 50% Analysis Date = 07/13/16 Pct Recovery = 50% Analysis Date = 07/09/16 Pct Recovery = 50% Analysis Date = 07/09/16 Pct Recovery = 50% Analysis Date = 07/04/16 Pct Recovery = 50% Analysis Date = 07/04/16 Pct Recovery = 50% Analysis Date = 06/30/16 Pct Recovery = 50% Analysis Date = 06/30/16 Pct Recovery = 50% Analysis Date = 06/25/16 Pct Recovery = 50% Analysis Date = 06/25/16 Pct Recovery = 50% Analysis Date = 06/21/16 Pct Recovery = 50% Analysis Date = 06/21/16 Pct Recovery = 50% Analysis Date = 06/16/16 Pct Recovery = 51% Analysis Date = 06/16/16 Pct Recovery = 51% Analysis Date = 06/12/16 Pct Recovery = 51% Analysis Date = 06/12/16 Pct Recovery = 51% Analysis Date = 06/07/16 Pct Recovery = 51% Analysis Date = 06/07/16 Pct Recovery = 51% Analysis Date = 06/03/16 Pct Recovery = 51% Analysis Date = 06/03/16 Pct Recovery = 51% Analysis Date = 05/29/16 Pct Recovery = 51% Analysis Date = 05/29/16 Pct Recovery = 51% Analysis Date = 05/25/16 Pct Recovery = 51% Analysis Date = 05/25/16 Pct Recovery = 51% Analysis Date = 05/20/16 Pct Recovery = 51% Analysis Date = 05/20/16 Pct Recovery = 51% Analysis Date = 05/16/16 Pct Recovery = 51% Analysis Date = 05/16/16 Pct Recovery = 51% Analysis Date = 05/11/16 Pct Recovery = 51% Analysis Date = 05/11/16 Pct Recovery = 51% Analysis Date = 05/07/16 Pct Recovery = 51% Analysis Date = 05/07/16 Pct Recovery = 51% Analysis Date = 05/02/16 Pct Recovery = 51% Analysis Date = 05/02/16 Pct Recovery = 51% Analysis Date = 04/28/16 Pct Recovery = 51% Analysis Date = 04/28/16 Pct Recovery = 51% Analysis Date = 04/23/16 Pct Recovery = 51% Analysis Date = 04/23/16 Pct Recovery = 51% Analysis Date = 04/19/16 Pct Recovery = 51% Analysis Date = 04/19/16 Pct Recovery = 51% Analysis Date = 04/14/16 Pct Recovery = 51% Analysis Date = 04/14/16 Pct Recovery = 51% Analysis Date = 04/10/16 Pct Recovery = 52% Analysis Date = 04/10/16 Pct Recovery = 52% Analysis Date = 04/05/16 Pct Recovery = 52% Analysis Date = 04/05/16 Pct Recovery = 52% Analysis Date = 04/01/16 Pct Recovery = 52% Analysis Date = 04/01/16 Pct Recovery = 52% Analysis Date = 03/27/16 Pct Recovery = 52% Analysis Date = 03/27/16 Pct Recovery = 52% Analysis Date = 03/23/16 Pct Recovery = 52% Analysis Date = 03/23/16 Pct Recovery = 52% Analysis Date = 03/18/16 Pct Recovery = 52% Analysis Date = 03/18/16 Pct Recovery = 52% Analysis Date = 03/14/16 Pct Recovery = 52% Analysis Date = 03/14/16 Pct Recovery = 52% Analysis Date = 03/09/16 Pct Recovery = 52% Analysis Date = 03/09/16 Pct Recovery = 52% Analysis Date = 03/05/16 Pct Recovery = 52% Analysis Date = 03/05/16 Pct Recovery = 52% Analysis Date = 02/29/16 Pct Recovery = 52% Analysis Date = 02/29/16 Pct Recovery = 52% Analysis Date = 02/25/16 Pct Recovery = 52% Analysis Date = 02/25/16 Pct Recovery = 52% Analysis Date = 02/20/16 Pct Recovery = 53% Analysis Date = 02/20/16 Pct Recovery = 53% Analysis Date = 02/16/16 Pct Recovery = 52% Analysis Date = 02/16/16 Pct Recovery = 52% Analysis Date = 02/11/16 Pct Recovery = 52% Analysis Date = 02/11/16 Pct Recovery = 52% Analysis Date = 02/07/16 Pct Recovery = 52% Analysis Date = 02/07/16 Pct Recovery = 52% Analysis Date = 02/02/16 Pct Recovery = 52% Analysis Date = 02/02/16 Pct Recovery = 52% Analysis Date = 01/29/16 Pct Recovery = 52% Analysis Date = 01/29/16 Pct Recovery = 52% Analysis Date = 01/24/16 Pct Recovery = 52% Analysis Date = 01/24/16 Pct Recovery = 52% Analysis Date = 01/20/16 Pct Recovery = 52% Analysis Date = 01/20/16 Pct Recovery = 52% Analysis Date = 01/15/16 Pct Recovery = 52% Analysis Date = 01/15/16 Pct Recovery = 52% Analysis Date = 01/11/16 Pct Recovery = 52% Analysis Date = 01/11/16 Pct Recovery = 52% Analysis Date = 01/06/16 Pct Recovery = 52% Analysis Date = 01/06/16 Pct Recovery = 52% Analysis Date = 01/02/16 Pct Recovery = 52% Analysis Date = 01/02/16 Pct Recovery = 52% Analysis Date = 12/28/15 Pct Recovery = 52% Analysis Date = 12/28/15 Pct Recovery = 52% Analysis Date = 12/24/15 Pct Recovery = 52% Analysis Date = 12/24/15 Pct Recovery = 52% Analysis Date = 12/19/15 Pct Recovery = 52% Analysis Date = 12/19/15 Pct Recovery = 52% Analysis Date = 12/15/15 Pct Recovery = 52% Analysis Date = 12/15/15 Pct Recovery = 52% Analysis Date = 12/10/15 Pct Recovery = 51% Analysis Date = 12/10/15 Pct Recovery = 51% Analysis Date = 12/06/15 Pct Recovery = 51% Analysis Date = 12/06/15 Pct Recovery = 51% Analysis Date = 12/01/15 Pct Recovery = 51% Analysis Date = 12/01/15 Pct Recovery = 51% Analysis Date = 11/27/15 Pct Recovery = 51% Analysis Date = 11/27/15 Pct Recovery = 51% Analysis Date = 11/22/15 Pct Recovery = 51% Analysis Date = 11/22/15 Pct Recovery = 51% Analysis Date = 11/18/15 Pct Recovery = 51% Analysis Date = 11/18/15 Pct Recovery = 51% Analysis Date = 11/13/15 Pct Recovery = 51% Analysis Date = 11/13/15 Pct Recovery = 51% Analysis Date = 11/09/15 Pct Recovery = 51% Analysis Date = 11/09/15 Pct Recovery = 51% Analysis Date = 11/04/15 Pct Recovery = 51% Analysis Date = 11/04/15 Pct Recovery = 51% Analysis Date = 10/31/15 Pct Recovery = 51% Analysis Date = 10/31/15 Pct Recovery = 51% Analysis Date = 10/26/15 Pct Recovery = 51% Analysis Date = 10/26/15 Pct Recovery = 51% Analysis Date = 10/22/15 Pct Recovery = 51% Analysis Date = 10/22/15 Pct Recovery = 51% Analysis Date = 10/17/15 Pct Recovery = 51% Analysis Date = 10/17/15 Pct Recovery = 51% Analysis Date = 10/13/15 Pct Recovery = 51% Analysis Date = 10/13/15 Pct Recovery = 51% Analysis Date = 10/08/15 Pct Recovery = 51% Analysis Date = 10/08/15 Pct Recovery = 51% Analysis Date = 10/04/15 Pct Recovery = 51% Analysis Date = 10/04/15 Pct Recovery = 51% Analysis Date = 09/29/15 Pct Recovery = 51% Analysis Date = 09/29/15 Pct Recovery = 51% Analysis Date = 09/25/15 Pct Recovery = 51% Analysis Date = 09/25/15 Pct Recovery = 51% Analysis Date = 09/20/15 Pct Recovery = 51% Analysis Date = 09/20/15 Pct Recovery = 51% Analysis Date = 09/16/15 Pct Recovery = 51% Analysis Date = 09/16/15 Pct Recovery = 51% Analysis Date = 09/11/15 Pct Recovery = 51% Analysis Date = 09/11/15 Pct Recovery = 51% Analysis Date = 09/07/15 Pct Recovery = 51% Analysis Date = 09/07/15 Pct Recovery = 51% Analysis Date = 09/02/15 Pct Recovery = 52% Analysis Date = 09/02/15 Pct Recovery = 52% Analysis Date = 08/29/15 Pct Recovery = 52% Analysis Date = 08/29/15 Pct Recovery = 52% Analysis Date = 08/24/15 Pct Recovery = 52% Analysis Date = 08/24/15 Pct Recovery = 52% Analysis Date = 08/20/15 Pct Recovery = 52% Analysis Date = 08/20/15 Pct Recovery = 52% Analysis Date = 08/15/15 Pct Recovery = 52% Analysis Date = 08/15/15 Pct Recovery = 52% Analysis Date = 08/11/15 Pct Recovery = 52% Analysis Date = 08/11/15 Pct Recovery = 52% Analysis Date = 08/06/15 Pct Recovery = 52% Analysis Date = 08/06/15 Pct Recovery = 52% Analysis Date = 08/02/15 Pct Recovery = 52% Analysis Date = 08/02/15 Pct Recovery = 52% Analysis Date = 07/28/15 Pct Recovery = 52% Analysis Date = 07/28/15 Pct Recovery = 52% Analysis Date = 07/24/15 Pct Recovery = 52% Analysis Date = 07/24/15 Pct Recovery = 52% Analysis Date = 07/19/15 Pct Recovery = 52% Analysis Date = 07/19/15 Pct Recovery = 52% Analysis Date = 07/15/15 Pct Recovery = 52% Analysis Date = 07/15/15 Pct Recovery = 52% Analysis Date = 07/10/15 Pct Recovery = 52% Analysis Date = 07/10/15 Pct Recovery = 52% Analysis Date = 07/06/15 Pct Recovery = 52% Analysis Date = 07/06/15 Pct Recovery = 52% Analysis Date = 07/01/15 Pct Recovery = 52% Analysis Date = 07/01/15 Pct Recovery = 52% Analysis Date = 06/27/15 Pct Recovery = 52% Analysis Date = 06/27/15 Pct Recovery = 52% Analysis Date = 06/22/15 Pct Recovery = 52% Analysis Date = 06/22/15 Pct Recovery = 52% Analysis Date = 06/18/15 Pct Recovery = 52% Analysis Date = 06/18/15 Pct Recovery = 52% Analysis Date = 06/13/15 Pct Recovery = 51% Analysis Date = 06/13/15 Pct Recovery = 51% Analysis Date = 06/09/15 Pct Recovery = 51% Analysis Date = 06/09/15 Pct Recovery = 51% Analysis Date = 06/04/15 Pct Recovery = 51% Analysis Date = 06/04/15 Pct Recovery = 51% Analysis Date = 05/31/15 Pct Recovery = 51% Analysis Date = 05/31/15 Pct Recovery = 51% Analysis Date = 05/26/15 Pct Recovery = 51% Analysis Date = 05/26/15 Pct Recovery = 51% Analysis Date = 05/22/15 Pct Recovery = 51% Analysis Date = 05/22/15 Pct Recovery = 51% Analysis Date = 05/17/15 Pct Recovery = 51% Analysis Date = 05/17/15 Pct Recovery = 51% Analysis Date = 05/13/15 Pct Recovery = 51% Analysis Date = 05/13/15 Pct Recovery = 51% Analysis Date = 05/08/15 Pct Recovery = 51% Analysis Date = 05/08/15 Pct Recovery = 51% Analysis Date = 05/04/15 Pct Recovery = 51% Analysis Date = 05/04/15 Pct Recovery = 51% Analysis Date = 04/29/15 Pct Recovery = 51% Analysis Date = 04/29/15 Pct Recovery = 51% Analysis Date = 04/25/15 Pct Recovery = 51% Analysis Date = 04/25/15 Pct Recovery = 51% Analysis Date = 04/20/15 Pct Recovery = 51% Analysis Date = 04/20/15 Pct Recovery = 51% Analysis Date = 04/16/15 Pct Recovery = 51% Analysis Date = 04/16/15 Pct Recovery = 51% Analysis Date = 04/11/15 Pct Recovery = 51% Analysis Date = 04/11/15 Pct Recovery = 51% Analysis Date = 04/07/15 Pct Recovery = 51% Analysis Date = 04/07/15 Pct Recovery = 51% Analysis Date = 04/02/15 Pct Recovery = 51% Analysis Date = 04/02/15 Pct Recovery = 51% Analysis Date = 03/29/15 Pct Recovery = 51% Analysis Date = 03/29/15 Pct Recovery = 51% Analysis Date = 03/24/15 Pct Recovery = 51% Analysis Date = 03/24/15 Pct Recovery = 51% Analysis Date = 03/20/15 Pct Recovery = 50% Analysis Date = 03/20/15 Pct Recovery = 50% Analysis Date = 03/15/15 Pct Recovery = 50% Analysis Date = 03/15/15 Pct Recovery = 50% Analysis Date = 03/11/15 Pct Recovery = 50% Analysis Date = 03/11/15 Pct Recovery = 50% Analysis Date = 03/06/15 Pct Recovery = 50% Analysis Date = 03/06/15 Pct Recovery = 50% Analysis Date = 03/02/15 Pct Recovery = 50% Analysis Date = 03/02/15 Pct Recovery = 50% Analysis Date = 02/25/15 Pct Recovery = 50% Analysis Date = 02/25/15 Pct Recovery = 50% Analysis Date = 02/21/15 Pct Recovery = 50% Analysis Date = 02/21/15 Pct Recovery = 50% Analysis Date = 02/16/15 Pct Recovery = 50% Analysis Date = 02/16/15 Pct Recovery = 50% Analysis Date = 02/12/15 Pct Recovery = 50% Analysis Date = 02/12/15 Pct Recovery = 50% Analysis Date = 02/07/15 Pct Recovery = 50% Analysis Date = 02/07/15 Pct Recovery = 50% Analysis Date = 02/03/15 Pct Recovery = 50% Analysis Date = 02/03/15 Pct Recovery = 50% Analysis Date = 01/29/15 Pct Recovery = 50% Analysis Date = 01/29/15 Pct Recovery = 50% Analysis Date = 01/25/15 Pct Recovery = 50% Analysis Date = 01/25/15 Pct Recovery = 50% Analysis Date = 01/20/15 Pct Recovery = 50% Analysis Date = 01/20/15 Pct Recovery = 50% Analysis Date = 01/16/15 Pct Recovery = 50% Analysis Date = 01/16/15 Pct Recovery = 50% Analysis Date = 01/11/15 Pct Recovery = 50% Analysis Date = 01/11/15 Pct Recovery = 50% Analysis Date = 01/07/15 Pct Recovery = 50% Analysis Date = 01/07/15 Pct Recovery = 50% Analysis Date = 01/02/15 Pct Recovery = 50% Analysis Date = 01/02/15 Pct Recovery = 50% Analysis Date = 12/29/14 Pct Recovery = 50% Analysis Date = 12/29/14 Pct Recovery = 50% Analysis Date = 12/24/14 Pct Recovery = 49% Analysis Date = 12/24/14 Pct Recovery = 49% Analysis Date = 12/20/14 Pct Recovery = 49% Analysis Date = 12/20/14 Pct Recovery = 49% Analysis Date = 12/15/14 Pct Recovery = 49% Analysis Date = 12/15/14 Pct Recovery = 49% Analysis Date = 12/11/14 Pct Recovery = 49% Analysis Date = 12/11/14 Pct Recovery = 49% Analysis Date = 12/06/14 Pct Recovery = 49% Analysis Date = 12/06/14 Pct Recovery = 49% Analysis Date = 12/02/14 Pct Recovery = 49% Analysis Date = 12/02/14 Pct Recovery = 49% Analysis Date = 11/27/14 Pct Recovery = 49% Analysis Date = 11/27/14 Pct Recovery = 49% Analysis Date = 11/23/14 Pct Recovery = 49% Analysis Date = 11/23/14 Pct Recovery = 49% Analysis Date = 11/18/14 Pct Recovery = 49% Analysis Date = 11/18/14 Pct Recovery = 49% Analysis Date = 11/14/14 Pct Recovery = 49% Analysis Date = 11/14/14 Pct Recovery = 49% Analysis Date = 11/09/14 Pct Recovery = 49% Analysis Date = 11/09/14 Pct Recovery = 49% Analysis Date = 11/05/14 Pct Recovery = 49% Analysis Date = 11/05/14 Pct Recovery = 49% Analysis Date = 10/31/14 Pct Recovery = 49% Analysis Date = 10/31/14 Pct Recovery = 49% Analysis Date = 10/27/14 Pct Recovery = 49% Analysis Date = 10/27/14 Pct Recovery = 49% Analysis Date = 10/22/14 Pct Recovery = 49% Analysis Date = 10/22/14 Pct Recovery = 49% Analysis Date = 10/18/14 Pct Recovery = 49% Analysis Date = 10/18/14 Pct Recovery = 49% Analysis Date = 10/13/14 Pct Recovery = 49% Analysis Date = 10/13/14 Pct Recovery = 49% Analysis Date = 10/09/14 Pct Recovery = 49% Analysis Date = 10/09/14 Pct Recovery = 49% Analysis Date = 10/04/14 Pct Recovery = 49% Analysis Date = 10/04/14 Pct Recovery = 49% Analysis Date = 09/30/14 Pct Recovery = 49% Analysis Date = 09/30/14 Pct Recovery = 49% Analysis Date = 09/25/14 Pct Recovery = 49% Analysis Date = 09/25/14 Pct Recovery = 49% Analysis Date = 09/21/14 Pct Recovery = 49% Analysis Date = 09/21/14 Pct Recovery = 49% Analysis Date = 09/16/14 Pct Recovery = 48% Analysis Date = 09/16/14 Pct Recovery = 48% Analysis Date = 09/12/14 Pct Recovery = 48% Analysis Date = 09/12/14 Pct Recovery = 48% Analysis Date = 09/07/14 Pct Recovery = 48% Analysis Date = 09/07/14 Pct Recovery = 48% Analysis Date = 09/03/14 Pct Recovery = 48% Analysis Date = 09/03/14 Pct Recovery = 48% Analysis Date = 08/29/14 Pct Recovery = 48% Analysis Date = 08/29/14 Pct Recovery = 48% Analysis Date = 08/25/14 Pct Recovery = 48% Analysis Date = 08/25/14 Pct Recovery = 48% Analysis Date = 08/20/14 Pct Recovery = 48% Analysis Date = 08/20/14 Pct Recovery = 48% Analysis Date = 08/16/14 Pct Recovery = 48% Analysis Date = 08/16/14 Pct Recovery = 48% Analysis Date = 08/11/14 Pct Recovery = 48% Analysis Date = 08/11/14 Pct Recovery = 48% Analysis Date = 08/07/14 Pct Recovery = 48% Analysis Date = 08/07/14 Pct Recovery = 48% Analysis Date = 08/02/14 Pct Recovery = 48% Analysis Date = 08/02/14 Pct Recovery = 48% Analysis Date = 07/29/14 Pct Recovery = 48% Analysis Date = 07/29/14 Pct Recovery = 48% Analysis Date = 07/24/14 Pct Recovery = 48% Analysis Date = 07/24/14 Pct Recovery = 48% Analysis Date = 07/20/14 Pct Recovery = 48% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
OSELTAMIVIR

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 57 51% 12% 51% 10%
Total 57 51% 12% 51% 10%

Sample Statistics
OSELTAMIVIR

Characteristic N % % Basis
Plotted 57 92% Spiked
Estimated Values 10 16% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 2 3% Spiked
Spiked 62 .  
False Negatives 3 5% 3 out of 62
Not Spiked 53 .  
False Positives 0 0% 0 out of 53

BQS OBSP Determination:
OXAZEPAM
METHOD: 2440 , TESTIDCODE: 67469LCM56
Open Data Set

Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 92% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 90% Analysis Date = 11/24/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 89% Analysis Date = 11/18/16 SpikeMix = ERA 04281604: 80 µl & ERA 04281603: 80 µl Pct Recovery = 84% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & ERA 04281604: 80 µl Pct Recovery = 88% Analysis Date = 09/24/16 SpikeMix = Crescent EN160610015: 80 µl & Abs 061416: 80 µl Pct Recovery = 33% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 42% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 51% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 45% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 41% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 46% Analysis Date = 12/07/14 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 44% Analysis Date = 10/25/14 SpikeMix = Abs 041614: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 36% Analysis Date = 06/22/14 SpikeMix = Abs 041814: 60 µl & Abs 041614: 60 µl Pct Recovery = 76% Analysis Date = 06/11/14 SpikeMix = Abs 041614: 60 µl & Abs 041714: 60 µl Pct Recovery = 56% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 93% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 80% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-07A: 40 µl & Abs 051315: 40 µl Pct Recovery = 83% Analysis Date = 07/31/15 SpikeMix = Abs 051315: 40 µl & Abs 052215: 40 µl Pct Recovery = 81% Analysis Date = 07/30/15 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 103% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 120% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 141% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 97% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 105% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 88% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 95% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 32% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 32% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 33% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 34% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 30% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 31% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 32% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 33% Analysis Date = 04/30/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 74% Analysis Date = 02/10/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 45% Analysis Date = 10/24/14 SpikeMix = ERA 0319-14-05: 8 µl & Abs 041614: 8 µl Pct Recovery = 29% Analysis Date = 04/23/14 SpikeMix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.2: 20 µl Pct Recovery = 80% Analysis Date = 09/12/14 SpikeMix = Abs 041614: 30 µl & ERA 0319-14-04: 30 µl Pct Recovery = 39% Analysis Date = 07/13/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 40% Analysis Date = 05/17/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 29% Analysis Date = 02/23/16 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 39% Analysis Date = 08/11/15 SpikeMix = Abs 050115: 20 µl & Abs 051315: 20 µl Pct Recovery = 70% Analysis Date = 06/09/15 SpikeMix = Abs 051315: 20 µl & Abs 050115: 20 µl Pct Recovery = 57% Analysis Date = 01/04/17 Pct Recovery = 96% Analysis Date = 12/31/16 Pct Recovery = 94% Analysis Date = 12/31/16 Pct Recovery = 94% Analysis Date = 12/26/16 Pct Recovery = 92% Analysis Date = 12/26/16 Pct Recovery = 92% Analysis Date = 12/21/16 Pct Recovery = 91% Analysis Date = 12/21/16 Pct Recovery = 91% Analysis Date = 12/16/16 Pct Recovery = 89% Analysis Date = 12/16/16 Pct Recovery = 89% Analysis Date = 12/11/16 Pct Recovery = 87% Analysis Date = 12/11/16 Pct Recovery = 87% Analysis Date = 12/06/16 Pct Recovery = 86% Analysis Date = 12/06/16 Pct Recovery = 86% Analysis Date = 12/01/16 Pct Recovery = 84% Analysis Date = 12/01/16 Pct Recovery = 84% Analysis Date = 11/26/16 Pct Recovery = 83% Analysis Date = 11/26/16 Pct Recovery = 83% Analysis Date = 11/21/16 Pct Recovery = 81% Analysis Date = 11/21/16 Pct Recovery = 81% Analysis Date = 11/16/16 Pct Recovery = 79% Analysis Date = 11/16/16 Pct Recovery = 79% Analysis Date = 11/11/16 Pct Recovery = 78% Analysis Date = 11/11/16 Pct Recovery = 78% Analysis Date = 11/06/16 Pct Recovery = 76% Analysis Date = 11/06/16 Pct Recovery = 76% Analysis Date = 11/01/16 Pct Recovery = 75% Analysis Date = 11/01/16 Pct Recovery = 75% Analysis Date = 10/27/16 Pct Recovery = 73% Analysis Date = 10/27/16 Pct Recovery = 73% Analysis Date = 10/22/16 Pct Recovery = 72% Analysis Date = 10/22/16 Pct Recovery = 72% Analysis Date = 10/17/16 Pct Recovery = 70% Analysis Date = 10/17/16 Pct Recovery = 70% Analysis Date = 10/13/16 Pct Recovery = 69% Analysis Date = 10/13/16 Pct Recovery = 69% Analysis Date = 10/08/16 Pct Recovery = 67% Analysis Date = 10/08/16 Pct Recovery = 67% Analysis Date = 10/03/16 Pct Recovery = 66% Analysis Date = 10/03/16 Pct Recovery = 66% Analysis Date = 09/28/16 Pct Recovery = 64% Analysis Date = 09/28/16 Pct Recovery = 64% Analysis Date = 09/23/16 Pct Recovery = 63% Analysis Date = 09/23/16 Pct Recovery = 63% Analysis Date = 09/18/16 Pct Recovery = 62% Analysis Date = 09/18/16 Pct Recovery = 62% Analysis Date = 09/13/16 Pct Recovery = 60% Analysis Date = 09/13/16 Pct Recovery = 60% Analysis Date = 09/08/16 Pct Recovery = 59% Analysis Date = 09/08/16 Pct Recovery = 59% Analysis Date = 09/03/16 Pct Recovery = 58% Analysis Date = 09/03/16 Pct Recovery = 58% Analysis Date = 08/29/16 Pct Recovery = 57% Analysis Date = 08/29/16 Pct Recovery = 57% Analysis Date = 08/24/16 Pct Recovery = 56% Analysis Date = 08/24/16 Pct Recovery = 56% Analysis Date = 08/19/16 Pct Recovery = 55% Analysis Date = 08/19/16 Pct Recovery = 55% Analysis Date = 08/14/16 Pct Recovery = 54% Analysis Date = 08/14/16 Pct Recovery = 54% Analysis Date = 08/09/16 Pct Recovery = 54% Analysis Date = 08/09/16 Pct Recovery = 54% Analysis Date = 08/04/16 Pct Recovery = 54% Analysis Date = 08/04/16 Pct Recovery = 54% Analysis Date = 07/30/16 Pct Recovery = 53% Analysis Date = 07/30/16 Pct Recovery = 53% Analysis Date = 07/25/16 Pct Recovery = 53% Analysis Date = 07/25/16 Pct Recovery = 53% Analysis Date = 07/21/16 Pct Recovery = 53% Analysis Date = 07/21/16 Pct Recovery = 53% Analysis Date = 07/16/16 Pct Recovery = 53% Analysis Date = 07/16/16 Pct Recovery = 53% Analysis Date = 07/11/16 Pct Recovery = 54% Analysis Date = 07/11/16 Pct Recovery = 54% Analysis Date = 07/06/16 Pct Recovery = 54% Analysis Date = 07/06/16 Pct Recovery = 54% Analysis Date = 07/01/16 Pct Recovery = 55% Analysis Date = 07/01/16 Pct Recovery = 55% Analysis Date = 06/26/16 Pct Recovery = 55% Analysis Date = 06/26/16 Pct Recovery = 55% Analysis Date = 06/21/16 Pct Recovery = 55% Analysis Date = 06/21/16 Pct Recovery = 55% Analysis Date = 06/16/16 Pct Recovery = 56% Analysis Date = 06/16/16 Pct Recovery = 56% Analysis Date = 06/11/16 Pct Recovery = 56% Analysis Date = 06/11/16 Pct Recovery = 56% Analysis Date = 06/06/16 Pct Recovery = 56% Analysis Date = 06/06/16 Pct Recovery = 56% Analysis Date = 06/01/16 Pct Recovery = 57% Analysis Date = 06/01/16 Pct Recovery = 57% Analysis Date = 05/27/16 Pct Recovery = 57% Analysis Date = 05/27/16 Pct Recovery = 57% Analysis Date = 05/22/16 Pct Recovery = 58% Analysis Date = 05/22/16 Pct Recovery = 58% Analysis Date = 05/17/16 Pct Recovery = 58% Analysis Date = 05/17/16 Pct Recovery = 58% Analysis Date = 05/12/16 Pct Recovery = 58% Analysis Date = 05/12/16 Pct Recovery = 58% Analysis Date = 05/07/16 Pct Recovery = 59% Analysis Date = 05/07/16 Pct Recovery = 59% Analysis Date = 05/02/16 Pct Recovery = 59% Analysis Date = 05/02/16 Pct Recovery = 59% Analysis Date = 04/28/16 Pct Recovery = 60% Analysis Date = 04/28/16 Pct Recovery = 60% Analysis Date = 04/23/16 Pct Recovery = 60% Analysis Date = 04/23/16 Pct Recovery = 60% Analysis Date = 04/18/16 Pct Recovery = 60% Analysis Date = 04/18/16 Pct Recovery = 60% Analysis Date = 04/13/16 Pct Recovery = 61% Analysis Date = 04/13/16 Pct Recovery = 61% Analysis Date = 04/08/16 Pct Recovery = 61% Analysis Date = 04/08/16 Pct Recovery = 61% Analysis Date = 04/03/16 Pct Recovery = 61% Analysis Date = 04/03/16 Pct Recovery = 61% Analysis Date = 03/29/16 Pct Recovery = 62% Analysis Date = 03/29/16 Pct Recovery = 62% Analysis Date = 03/24/16 Pct Recovery = 62% Analysis Date = 03/24/16 Pct Recovery = 62% Analysis Date = 03/19/16 Pct Recovery = 63% Analysis Date = 03/19/16 Pct Recovery = 63% Analysis Date = 03/14/16 Pct Recovery = 63% Analysis Date = 03/14/16 Pct Recovery = 63% Analysis Date = 03/09/16 Pct Recovery = 63% Analysis Date = 03/09/16 Pct Recovery = 63% Analysis Date = 03/04/16 Pct Recovery = 64% Analysis Date = 03/04/16 Pct Recovery = 64% Analysis Date = 02/28/16 Pct Recovery = 64% Analysis Date = 02/28/16 Pct Recovery = 64% Analysis Date = 02/23/16 Pct Recovery = 65% Analysis Date = 02/23/16 Pct Recovery = 65% Analysis Date = 02/18/16 Pct Recovery = 65% Analysis Date = 02/18/16 Pct Recovery = 65% Analysis Date = 02/13/16 Pct Recovery = 65% Analysis Date = 02/13/16 Pct Recovery = 65% Analysis Date = 02/09/16 Pct Recovery = 66% Analysis Date = 02/09/16 Pct Recovery = 66% Analysis Date = 02/04/16 Pct Recovery = 66% Analysis Date = 02/04/16 Pct Recovery = 66% Analysis Date = 01/30/16 Pct Recovery = 66% Analysis Date = 01/30/16 Pct Recovery = 66% Analysis Date = 01/25/16 Pct Recovery = 67% Analysis Date = 01/25/16 Pct Recovery = 67% Analysis Date = 01/20/16 Pct Recovery = 67% Analysis Date = 01/20/16 Pct Recovery = 67% Analysis Date = 01/15/16 Pct Recovery = 68% Analysis Date = 01/15/16 Pct Recovery = 68% Analysis Date = 01/10/16 Pct Recovery = 68% Analysis Date = 01/10/16 Pct Recovery = 68% Analysis Date = 01/05/16 Pct Recovery = 68% Analysis Date = 01/05/16 Pct Recovery = 68% Analysis Date = 12/31/15 Pct Recovery = 69% Analysis Date = 12/31/15 Pct Recovery = 69% Analysis Date = 12/26/15 Pct Recovery = 69% Analysis Date = 12/26/15 Pct Recovery = 69% Analysis Date = 12/21/15 Pct Recovery = 70% Analysis Date = 12/21/15 Pct Recovery = 70% Analysis Date = 12/16/15 Pct Recovery = 70% Analysis Date = 12/16/15 Pct Recovery = 70% Analysis Date = 12/11/15 Pct Recovery = 70% Analysis Date = 12/11/15 Pct Recovery = 70% Analysis Date = 12/06/15 Pct Recovery = 71% Analysis Date = 12/06/15 Pct Recovery = 71% Analysis Date = 12/01/15 Pct Recovery = 71% Analysis Date = 12/01/15 Pct Recovery = 71% Analysis Date = 11/26/15 Pct Recovery = 71% Analysis Date = 11/26/15 Pct Recovery = 71% Analysis Date = 11/21/15 Pct Recovery = 72% Analysis Date = 11/21/15 Pct Recovery = 72% Analysis Date = 11/17/15 Pct Recovery = 71% Analysis Date = 11/17/15 Pct Recovery = 71% Analysis Date = 11/12/15 Pct Recovery = 71% Analysis Date = 11/12/15 Pct Recovery = 71% Analysis Date = 11/07/15 Pct Recovery = 71% Analysis Date = 11/07/15 Pct Recovery = 71% Analysis Date = 11/02/15 Pct Recovery = 71% Analysis Date = 11/02/15 Pct Recovery = 71% Analysis Date = 10/28/15 Pct Recovery = 71% Analysis Date = 10/28/15 Pct Recovery = 71% Analysis Date = 10/23/15 Pct Recovery = 71% Analysis Date = 10/23/15 Pct Recovery = 71% Analysis Date = 10/18/15 Pct Recovery = 71% Analysis Date = 10/18/15 Pct Recovery = 71% Analysis Date = 10/13/15 Pct Recovery = 70% Analysis Date = 10/13/15 Pct Recovery = 70% Analysis Date = 10/08/15 Pct Recovery = 70% Analysis Date = 10/08/15 Pct Recovery = 70% Analysis Date = 10/03/15 Pct Recovery = 70% Analysis Date = 10/03/15 Pct Recovery = 70% Analysis Date = 09/28/15 Pct Recovery = 70% Analysis Date = 09/28/15 Pct Recovery = 70% Analysis Date = 09/23/15 Pct Recovery = 70% Analysis Date = 09/23/15 Pct Recovery = 70% Analysis Date = 09/18/15 Pct Recovery = 70% Analysis Date = 09/18/15 Pct Recovery = 70% Analysis Date = 09/13/15 Pct Recovery = 70% Analysis Date = 09/13/15 Pct Recovery = 70% Analysis Date = 09/08/15 Pct Recovery = 69% Analysis Date = 09/08/15 Pct Recovery = 69% Analysis Date = 09/03/15 Pct Recovery = 69% Analysis Date = 09/03/15 Pct Recovery = 69% Analysis Date = 08/29/15 Pct Recovery = 69% Analysis Date = 08/29/15 Pct Recovery = 69% Analysis Date = 08/25/15 Pct Recovery = 69% Analysis Date = 08/25/15 Pct Recovery = 69% Analysis Date = 08/20/15 Pct Recovery = 69% Analysis Date = 08/20/15 Pct Recovery = 69% Analysis Date = 08/15/15 Pct Recovery = 69% Analysis Date = 08/15/15 Pct Recovery = 69% Analysis Date = 08/10/15 Pct Recovery = 69% Analysis Date = 08/10/15 Pct Recovery = 69% Analysis Date = 08/05/15 Pct Recovery = 68% Analysis Date = 08/05/15 Pct Recovery = 68% Analysis Date = 07/31/15 Pct Recovery = 68% Analysis Date = 07/31/15 Pct Recovery = 68% Analysis Date = 07/26/15 Pct Recovery = 68% Analysis Date = 07/26/15 Pct Recovery = 68% Analysis Date = 07/21/15 Pct Recovery = 68% Analysis Date = 07/21/15 Pct Recovery = 68% Analysis Date = 07/16/15 Pct Recovery = 68% Analysis Date = 07/16/15 Pct Recovery = 68% Analysis Date = 07/11/15 Pct Recovery = 67% Analysis Date = 07/11/15 Pct Recovery = 67% Analysis Date = 07/06/15 Pct Recovery = 67% Analysis Date = 07/06/15 Pct Recovery = 67% Analysis Date = 07/01/15 Pct Recovery = 67% Analysis Date = 07/01/15 Pct Recovery = 67% Analysis Date = 06/26/15 Pct Recovery = 66% Analysis Date = 06/26/15 Pct Recovery = 66% Analysis Date = 06/21/15 Pct Recovery = 66% Analysis Date = 06/21/15 Pct Recovery = 66% Analysis Date = 06/16/15 Pct Recovery = 66% Analysis Date = 06/16/15 Pct Recovery = 66% Analysis Date = 06/11/15 Pct Recovery = 65% Analysis Date = 06/11/15 Pct Recovery = 65% Analysis Date = 06/07/15 Pct Recovery = 65% Analysis Date = 06/07/15 Pct Recovery = 65% Analysis Date = 06/02/15 Pct Recovery = 65% Analysis Date = 06/02/15 Pct Recovery = 65% Analysis Date = 05/28/15 Pct Recovery = 65% Analysis Date = 05/28/15 Pct Recovery = 65% Analysis Date = 05/23/15 Pct Recovery = 64% Analysis Date = 05/23/15 Pct Recovery = 64% Analysis Date = 05/18/15 Pct Recovery = 64% Analysis Date = 05/18/15 Pct Recovery = 64% Analysis Date = 05/13/15 Pct Recovery = 64% Analysis Date = 05/13/15 Pct Recovery = 64% Analysis Date = 05/08/15 Pct Recovery = 63% Analysis Date = 05/08/15 Pct Recovery = 63% Analysis Date = 05/03/15 Pct Recovery = 63% Analysis Date = 05/03/15 Pct Recovery = 63% Analysis Date = 04/28/15 Pct Recovery = 63% Analysis Date = 04/28/15 Pct Recovery = 63% Analysis Date = 04/23/15 Pct Recovery = 63% Analysis Date = 04/23/15 Pct Recovery = 63% Analysis Date = 04/18/15 Pct Recovery = 62% Analysis Date = 04/18/15 Pct Recovery = 62% Analysis Date = 04/13/15 Pct Recovery = 62% Analysis Date = 04/13/15 Pct Recovery = 62% Analysis Date = 04/08/15 Pct Recovery = 62% Analysis Date = 04/08/15 Pct Recovery = 62% Analysis Date = 04/03/15 Pct Recovery = 61% Analysis Date = 04/03/15 Pct Recovery = 61% Analysis Date = 03/29/15 Pct Recovery = 61% Analysis Date = 03/29/15 Pct Recovery = 61% Analysis Date = 03/24/15 Pct Recovery = 61% Analysis Date = 03/24/15 Pct Recovery = 61% Analysis Date = 03/19/15 Pct Recovery = 61% Analysis Date = 03/19/15 Pct Recovery = 61% Analysis Date = 03/15/15 Pct Recovery = 60% Analysis Date = 03/15/15 Pct Recovery = 60% Analysis Date = 03/10/15 Pct Recovery = 60% Analysis Date = 03/10/15 Pct Recovery = 60% Analysis Date = 03/05/15 Pct Recovery = 60% Analysis Date = 03/05/15 Pct Recovery = 60% Analysis Date = 02/28/15 Pct Recovery = 59% Analysis Date = 02/28/15 Pct Recovery = 59% Analysis Date = 02/23/15 Pct Recovery = 59% Analysis Date = 02/23/15 Pct Recovery = 59% Analysis Date = 02/18/15 Pct Recovery = 59% Analysis Date = 02/18/15 Pct Recovery = 59% Analysis Date = 02/13/15 Pct Recovery = 59% Analysis Date = 02/13/15 Pct Recovery = 59% Analysis Date = 02/08/15 Pct Recovery = 59% Analysis Date = 02/08/15 Pct Recovery = 59% Analysis Date = 02/03/15 Pct Recovery = 58% Analysis Date = 02/03/15 Pct Recovery = 58% Analysis Date = 01/29/15 Pct Recovery = 58% Analysis Date = 01/29/15 Pct Recovery = 58% Analysis Date = 01/24/15 Pct Recovery = 58% Analysis Date = 01/24/15 Pct Recovery = 58% Analysis Date = 01/19/15 Pct Recovery = 58% Analysis Date = 01/19/15 Pct Recovery = 58% Analysis Date = 01/14/15 Pct Recovery = 57% Analysis Date = 01/14/15 Pct Recovery = 57% Analysis Date = 01/09/15 Pct Recovery = 57% Analysis Date = 01/09/15 Pct Recovery = 57% Analysis Date = 01/04/15 Pct Recovery = 57% Analysis Date = 01/04/15 Pct Recovery = 57% Analysis Date = 12/30/14 Pct Recovery = 57% Analysis Date = 12/30/14 Pct Recovery = 57% Analysis Date = 12/25/14 Pct Recovery = 56% Analysis Date = 12/25/14 Pct Recovery = 56% Analysis Date = 12/21/14 Pct Recovery = 56% Analysis Date = 12/21/14 Pct Recovery = 56% Analysis Date = 12/16/14 Pct Recovery = 56% Analysis Date = 12/16/14 Pct Recovery = 56% Analysis Date = 12/11/14 Pct Recovery = 56% Analysis Date = 12/11/14 Pct Recovery = 56% Analysis Date = 12/06/14 Pct Recovery = 55% Analysis Date = 12/06/14 Pct Recovery = 55% Analysis Date = 12/01/14 Pct Recovery = 55% Analysis Date = 12/01/14 Pct Recovery = 55% Analysis Date = 11/26/14 Pct Recovery = 55% Analysis Date = 11/26/14 Pct Recovery = 55% Analysis Date = 11/21/14 Pct Recovery = 55% Analysis Date = 11/21/14 Pct Recovery = 55% Analysis Date = 11/16/14 Pct Recovery = 54% Analysis Date = 11/16/14 Pct Recovery = 54% Analysis Date = 11/11/14 Pct Recovery = 54% Analysis Date = 11/11/14 Pct Recovery = 54% Analysis Date = 11/06/14 Pct Recovery = 54% Analysis Date = 11/06/14 Pct Recovery = 54% Analysis Date = 11/01/14 Pct Recovery = 54% Analysis Date = 11/01/14 Pct Recovery = 54% Analysis Date = 10/27/14 Pct Recovery = 53% Analysis Date = 10/27/14 Pct Recovery = 53% Analysis Date = 10/22/14 Pct Recovery = 53% Analysis Date = 10/22/14 Pct Recovery = 53% Analysis Date = 10/17/14 Pct Recovery = 53% Analysis Date = 10/17/14 Pct Recovery = 53% Analysis Date = 10/12/14 Pct Recovery = 53% Analysis Date = 10/12/14 Pct Recovery = 53% Analysis Date = 10/07/14 Pct Recovery = 52% Analysis Date = 10/07/14 Pct Recovery = 52% Analysis Date = 10/03/14 Pct Recovery = 52% Analysis Date = 10/03/14 Pct Recovery = 52% Analysis Date = 09/28/14 Pct Recovery = 52% Analysis Date = 09/28/14 Pct Recovery = 52% Analysis Date = 09/23/14 Pct Recovery = 52% Analysis Date = 09/23/14 Pct Recovery = 52% Analysis Date = 09/18/14 Pct Recovery = 52% Analysis Date = 09/18/14 Pct Recovery = 52% Analysis Date = 09/13/14 Pct Recovery = 51% Analysis Date = 09/13/14 Pct Recovery = 51% Analysis Date = 09/08/14 Pct Recovery = 51% Analysis Date = 09/08/14 Pct Recovery = 51% Analysis Date = 09/03/14 Pct Recovery = 51% Analysis Date = 09/03/14 Pct Recovery = 51% Analysis Date = 08/29/14 Pct Recovery = 51% Analysis Date = 08/29/14 Pct Recovery = 51% Analysis Date = 08/24/14 Pct Recovery = 50% Analysis Date = 08/24/14 Pct Recovery = 50% Analysis Date = 08/19/14 Pct Recovery = 50% Analysis Date = 08/19/14 Pct Recovery = 50% Analysis Date = 08/14/14 Pct Recovery = 50% Analysis Date = 08/14/14 Pct Recovery = 50% Analysis Date = 08/09/14 Pct Recovery = 50% Analysis Date = 08/09/14 Pct Recovery = 50% Analysis Date = 08/04/14 Pct Recovery = 49% Analysis Date = 08/04/14 Pct Recovery = 49% Analysis Date = 07/30/14 Pct Recovery = 49% Analysis Date = 07/30/14 Pct Recovery = 49% Analysis Date = 07/25/14 Pct Recovery = 49% Analysis Date = 07/25/14 Pct Recovery = 49% Analysis Date = 07/20/14 Pct Recovery = 49% Analysis Date = 07/20/14 Pct Recovery = 49% Analysis Date = 07/15/14 Pct Recovery = 48% Analysis Date = 07/15/14 Pct Recovery = 48% Analysis Date = 07/11/14 Pct Recovery = 48% Analysis Date = 07/11/14 Pct Recovery = 48% Analysis Date = 07/06/14 Pct Recovery = 48% Analysis Date = 07/06/14 Pct Recovery = 48% Analysis Date = 07/01/14 Pct Recovery = 48% Analysis Date = 07/01/14 Pct Recovery = 48% Analysis Date = 06/26/14 Pct Recovery = 47% Analysis Date = 06/26/14 Pct Recovery = 47% Analysis Date = 06/21/14 Pct Recovery = 47% Analysis Date = 06/21/14 Pct Recovery = 47% Analysis Date = 06/16/14 Pct Recovery = 47% Analysis Date = 06/16/14 Pct Recovery = 47% Analysis Date = 06/11/14 Pct Recovery = 47% Analysis Date = 06/11/14 Pct Recovery = 47% Analysis Date = 06/06/14 Pct Recovery = 47% Analysis Date = 06/06/14 Pct Recovery = 47% Analysis Date = 06/01/14 Pct Recovery = 46% Analysis Date = 06/01/14 Pct Recovery = 46% Analysis Date = 05/27/14 Pct Recovery = 46% Analysis Date = 05/27/14 Pct Recovery = 46% Analysis Date = 05/22/14 Pct Recovery = 46% Analysis Date = 05/22/14 Pct Recovery = 46% Analysis Date = 05/17/14 Pct Recovery = 46% Analysis Date = 05/17/14 Pct Recovery = 46% Analysis Date = 05/12/14 Pct Recovery = 46% Analysis Date = 05/12/14 Pct Recovery = 46% Analysis Date = 05/07/14 Pct Recovery = 45% Analysis Date = 05/07/14 Pct Recovery = 45% Analysis Date = 05/02/14 Pct Recovery = 45% Analysis Date = 05/02/14 Pct Recovery = 45% Analysis Date = 04/27/14 Pct Recovery = 45% Analysis Date = 04/27/14 Pct Recovery = 45% Analysis Date = 04/23/14 Pct Recovery = 45% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
OXAZEPAM

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 44 63% 29% 53% 39%
Total 44 63% 29% 53% 39%

Sample Statistics
OXAZEPAM

Characteristic N % % Basis
Plotted 44 85% Spiked
Estimated Values 19 37% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 2 4% Spiked
Spiked 52 .  
False Negatives 6 12% 6 out of 52
Not Spiked 63 .  
False Positives 0 0% 0 out of 63

BQS OBSP Determination:
OXYCODONE
METHOD: 2440 , TESTIDCODE: 67495LCM56
Open Data Set

Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 72% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 73% Analysis Date = 11/24/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 78% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 80 µl & Abs 051315: 80 µl Pct Recovery = 68% Analysis Date = 10/01/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 66% Analysis Date = 09/24/16 SpikeMix = Crescent EN160610015: 80 µl & Abs 061416: 80 µl Pct Recovery = 66% Analysis Date = 09/24/16 SpikeMix = Abs 061416: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 62% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 79% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 84% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 83% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 84% Analysis Date = 11/18/16 SpikeMix = ERA 04281604: 80 µl & ERA 04281603: 80 µl Pct Recovery = 87% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & ERA 04281604: 80 µl Pct Recovery = 82% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-04: 15 µl & Abs 041814: 15 µl Pct Recovery = 69% Analysis Date = 02/06/15 SpikeMix = Abs 041814: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 60% Analysis Date = 07/12/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 76% Analysis Date = 06/22/14 SpikeMix = Abs 041814: 60 µl & Abs 041614: 60 µl Pct Recovery = 88% Analysis Date = 05/21/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 65% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 65% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 60% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-07A: 40 µl & Abs 051315: 40 µl Pct Recovery = 58% Analysis Date = 07/31/15 SpikeMix = Abs 051315: 40 µl & Abs 052215: 40 µl Pct Recovery = 77% Analysis Date = 07/30/15 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 84% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 83% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 83% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 74% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 73% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 75% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 82% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 89% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 95% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 126% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 147% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 96% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 92% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 71% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 67% Analysis Date = 04/10/15 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 91% Analysis Date = 11/04/14 SpikeMix = Abs 041814: 8 µl & ERA 0318-14-02: 8 µl Pct Recovery = 80% Analysis Date = 10/11/14 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 52% Analysis Date = 10/10/14 SpikeMix = Abs 041714: 30 µl & Abs 041814: 30 µl Pct Recovery = 56% Analysis Date = 10/10/14 SpikeMix = Abs 041814: 30 µl & ERA 0318-14-02: 30 µl Pct Recovery = 55% Analysis Date = 07/13/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 78% Analysis Date = 05/30/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 55% Analysis Date = 02/23/16 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 61% Analysis Date = 08/11/15 SpikeMix = Abs 050115: 20 µl & Abs 051315: 20 µl Pct Recovery = 70% Analysis Date = 06/26/15 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 64% Analysis Date = 01/04/17 Pct Recovery = 100% Analysis Date = 12/31/16 Pct Recovery = 99% Analysis Date = 12/31/16 Pct Recovery = 99% Analysis Date = 12/26/16 Pct Recovery = 98% Analysis Date = 12/26/16 Pct Recovery = 98% Analysis Date = 12/21/16 Pct Recovery = 98% Analysis Date = 12/21/16 Pct Recovery = 98% Analysis Date = 12/16/16 Pct Recovery = 97% Analysis Date = 12/16/16 Pct Recovery = 97% Analysis Date = 12/11/16 Pct Recovery = 96% Analysis Date = 12/11/16 Pct Recovery = 96% Analysis Date = 12/07/16 Pct Recovery = 95% Analysis Date = 12/07/16 Pct Recovery = 95% Analysis Date = 12/02/16 Pct Recovery = 94% Analysis Date = 12/02/16 Pct Recovery = 94% Analysis Date = 11/27/16 Pct Recovery = 93% Analysis Date = 11/27/16 Pct Recovery = 93% Analysis Date = 11/22/16 Pct Recovery = 93% Analysis Date = 11/22/16 Pct Recovery = 93% Analysis Date = 11/17/16 Pct Recovery = 92% Analysis Date = 11/17/16 Pct Recovery = 92% Analysis Date = 11/13/16 Pct Recovery = 91% Analysis Date = 11/13/16 Pct Recovery = 91% Analysis Date = 11/08/16 Pct Recovery = 90% Analysis Date = 11/08/16 Pct Recovery = 90% Analysis Date = 11/03/16 Pct Recovery = 90% Analysis Date = 11/03/16 Pct Recovery = 90% Analysis Date = 10/29/16 Pct Recovery = 89% Analysis Date = 10/29/16 Pct Recovery = 89% Analysis Date = 10/24/16 Pct Recovery = 88% Analysis Date = 10/24/16 Pct Recovery = 88% Analysis Date = 10/20/16 Pct Recovery = 87% Analysis Date = 10/20/16 Pct Recovery = 87% Analysis Date = 10/15/16 Pct Recovery = 86% Analysis Date = 10/15/16 Pct Recovery = 86% Analysis Date = 10/10/16 Pct Recovery = 86% Analysis Date = 10/10/16 Pct Recovery = 86% Analysis Date = 10/05/16 Pct Recovery = 85% Analysis Date = 10/05/16 Pct Recovery = 85% Analysis Date = 09/30/16 Pct Recovery = 84% Analysis Date = 09/30/16 Pct Recovery = 84% Analysis Date = 09/26/16 Pct Recovery = 83% Analysis Date = 09/26/16 Pct Recovery = 83% Analysis Date = 09/21/16 Pct Recovery = 83% Analysis Date = 09/21/16 Pct Recovery = 83% Analysis Date = 09/16/16 Pct Recovery = 82% Analysis Date = 09/16/16 Pct Recovery = 82% Analysis Date = 09/11/16 Pct Recovery = 81% Analysis Date = 09/11/16 Pct Recovery = 81% Analysis Date = 09/06/16 Pct Recovery = 81% Analysis Date = 09/06/16 Pct Recovery = 81% Analysis Date = 09/02/16 Pct Recovery = 80% Analysis Date = 09/02/16 Pct Recovery = 80% Analysis Date = 08/28/16 Pct Recovery = 79% Analysis Date = 08/28/16 Pct Recovery = 79% Analysis Date = 08/23/16 Pct Recovery = 79% Analysis Date = 08/23/16 Pct Recovery = 79% Analysis Date = 08/18/16 Pct Recovery = 78% Analysis Date = 08/18/16 Pct Recovery = 78% Analysis Date = 08/13/16 Pct Recovery = 77% Analysis Date = 08/13/16 Pct Recovery = 77% Analysis Date = 08/09/16 Pct Recovery = 77% Analysis Date = 08/09/16 Pct Recovery = 77% Analysis Date = 08/04/16 Pct Recovery = 76% Analysis Date = 08/04/16 Pct Recovery = 76% Analysis Date = 07/30/16 Pct Recovery = 76% Analysis Date = 07/30/16 Pct Recovery = 76% Analysis Date = 07/25/16 Pct Recovery = 75% Analysis Date = 07/25/16 Pct Recovery = 75% Analysis Date = 07/20/16 Pct Recovery = 75% Analysis Date = 07/20/16 Pct Recovery = 75% Analysis Date = 07/16/16 Pct Recovery = 75% Analysis Date = 07/16/16 Pct Recovery = 75% Analysis Date = 07/11/16 Pct Recovery = 75% Analysis Date = 07/11/16 Pct Recovery = 75% Analysis Date = 07/06/16 Pct Recovery = 75% Analysis Date = 07/06/16 Pct Recovery = 75% Analysis Date = 07/01/16 Pct Recovery = 74% Analysis Date = 07/01/16 Pct Recovery = 74% Analysis Date = 06/26/16 Pct Recovery = 74% Analysis Date = 06/26/16 Pct Recovery = 74% Analysis Date = 06/22/16 Pct Recovery = 74% Analysis Date = 06/22/16 Pct Recovery = 74% Analysis Date = 06/17/16 Pct Recovery = 74% Analysis Date = 06/17/16 Pct Recovery = 74% Analysis Date = 06/12/16 Pct Recovery = 74% Analysis Date = 06/12/16 Pct Recovery = 74% Analysis Date = 06/07/16 Pct Recovery = 74% Analysis Date = 06/07/16 Pct Recovery = 74% Analysis Date = 06/02/16 Pct Recovery = 73% Analysis Date = 06/02/16 Pct Recovery = 73% Analysis Date = 05/29/16 Pct Recovery = 73% Analysis Date = 05/29/16 Pct Recovery = 73% Analysis Date = 05/24/16 Pct Recovery = 73% Analysis Date = 05/24/16 Pct Recovery = 73% Analysis Date = 05/19/16 Pct Recovery = 73% Analysis Date = 05/19/16 Pct Recovery = 73% Analysis Date = 05/14/16 Pct Recovery = 73% Analysis Date = 05/14/16 Pct Recovery = 73% Analysis Date = 05/09/16 Pct Recovery = 73% Analysis Date = 05/09/16 Pct Recovery = 73% Analysis Date = 05/05/16 Pct Recovery = 72% Analysis Date = 05/05/16 Pct Recovery = 72% Analysis Date = 04/30/16 Pct Recovery = 72% Analysis Date = 04/30/16 Pct Recovery = 72% Analysis Date = 04/25/16 Pct Recovery = 72% Analysis Date = 04/25/16 Pct Recovery = 72% Analysis Date = 04/20/16 Pct Recovery = 72% Analysis Date = 04/20/16 Pct Recovery = 72% Analysis Date = 04/15/16 Pct Recovery = 72% Analysis Date = 04/15/16 Pct Recovery = 72% Analysis Date = 04/11/16 Pct Recovery = 72% Analysis Date = 04/11/16 Pct Recovery = 72% Analysis Date = 04/06/16 Pct Recovery = 71% Analysis Date = 04/06/16 Pct Recovery = 71% Analysis Date = 04/01/16 Pct Recovery = 71% Analysis Date = 04/01/16 Pct Recovery = 71% Analysis Date = 03/27/16 Pct Recovery = 71% Analysis Date = 03/27/16 Pct Recovery = 71% Analysis Date = 03/22/16 Pct Recovery = 71% Analysis Date = 03/22/16 Pct Recovery = 71% Analysis Date = 03/18/16 Pct Recovery = 71% Analysis Date = 03/18/16 Pct Recovery = 71% Analysis Date = 03/13/16 Pct Recovery = 71% Analysis Date = 03/13/16 Pct Recovery = 71% Analysis Date = 03/08/16 Pct Recovery = 70% Analysis Date = 03/08/16 Pct Recovery = 70% Analysis Date = 03/03/16 Pct Recovery = 70% Analysis Date = 03/03/16 Pct Recovery = 70% Analysis Date = 02/27/16 Pct Recovery = 70% Analysis Date = 02/27/16 Pct Recovery = 70% Analysis Date = 02/23/16 Pct Recovery = 70% Analysis Date = 02/23/16 Pct Recovery = 70% Analysis Date = 02/18/16 Pct Recovery = 70% Analysis Date = 02/18/16 Pct Recovery = 70% Analysis Date = 02/13/16 Pct Recovery = 70% Analysis Date = 02/13/16 Pct Recovery = 70% Analysis Date = 02/08/16 Pct Recovery = 70% Analysis Date = 02/08/16 Pct Recovery = 70% Analysis Date = 02/03/16 Pct Recovery = 70% Analysis Date = 02/03/16 Pct Recovery = 70% Analysis Date = 01/30/16 Pct Recovery = 70% Analysis Date = 01/30/16 Pct Recovery = 70% Analysis Date = 01/25/16 Pct Recovery = 70% Analysis Date = 01/25/16 Pct Recovery = 70% Analysis Date = 01/20/16 Pct Recovery = 70% Analysis Date = 01/20/16 Pct Recovery = 70% Analysis Date = 01/15/16 Pct Recovery = 70% Analysis Date = 01/15/16 Pct Recovery = 70% Analysis Date = 01/10/16 Pct Recovery = 70% Analysis Date = 01/10/16 Pct Recovery = 70% Analysis Date = 01/06/16 Pct Recovery = 70% Analysis Date = 01/06/16 Pct Recovery = 70% Analysis Date = 01/01/16 Pct Recovery = 70% Analysis Date = 01/01/16 Pct Recovery = 70% Analysis Date = 12/27/15 Pct Recovery = 70% Analysis Date = 12/27/15 Pct Recovery = 70% Analysis Date = 12/22/15 Pct Recovery = 70% Analysis Date = 12/22/15 Pct Recovery = 70% Analysis Date = 12/17/15 Pct Recovery = 70% Analysis Date = 12/17/15 Pct Recovery = 70% Analysis Date = 12/13/15 Pct Recovery = 70% Analysis Date = 12/13/15 Pct Recovery = 70% Analysis Date = 12/08/15 Pct Recovery = 70% Analysis Date = 12/08/15 Pct Recovery = 70% Analysis Date = 12/03/15 Pct Recovery = 70% Analysis Date = 12/03/15 Pct Recovery = 70% Analysis Date = 11/28/15 Pct Recovery = 70% Analysis Date = 11/28/15 Pct Recovery = 70% Analysis Date = 11/23/15 Pct Recovery = 70% Analysis Date = 11/23/15 Pct Recovery = 70% Analysis Date = 11/19/15 Pct Recovery = 70% Analysis Date = 11/19/15 Pct Recovery = 70% Analysis Date = 11/14/15 Pct Recovery = 70% Analysis Date = 11/14/15 Pct Recovery = 70% Analysis Date = 11/09/15 Pct Recovery = 70% Analysis Date = 11/09/15 Pct Recovery = 70% Analysis Date = 11/04/15 Pct Recovery = 70% Analysis Date = 11/04/15 Pct Recovery = 70% Analysis Date = 10/30/15 Pct Recovery = 70% Analysis Date = 10/30/15 Pct Recovery = 70% Analysis Date = 10/26/15 Pct Recovery = 70% Analysis Date = 10/26/15 Pct Recovery = 70% Analysis Date = 10/21/15 Pct Recovery = 70% Analysis Date = 10/21/15 Pct Recovery = 70% Analysis Date = 10/16/15 Pct Recovery = 70% Analysis Date = 10/16/15 Pct Recovery = 70% Analysis Date = 10/11/15 Pct Recovery = 70% Analysis Date = 10/11/15 Pct Recovery = 70% Analysis Date = 10/06/15 Pct Recovery = 70% Analysis Date = 10/06/15 Pct Recovery = 70% Analysis Date = 10/02/15 Pct Recovery = 71% Analysis Date = 10/02/15 Pct Recovery = 71% Analysis Date = 09/27/15 Pct Recovery = 71% Analysis Date = 09/27/15 Pct Recovery = 71% Analysis Date = 09/22/15 Pct Recovery = 70% Analysis Date = 09/22/15 Pct Recovery = 70% Analysis Date = 09/17/15 Pct Recovery = 70% Analysis Date = 09/17/15 Pct Recovery = 70% Analysis Date = 09/12/15 Pct Recovery = 70% Analysis Date = 09/12/15 Pct Recovery = 70% Analysis Date = 09/08/15 Pct Recovery = 70% Analysis Date = 09/08/15 Pct Recovery = 70% Analysis Date = 09/03/15 Pct Recovery = 70% Analysis Date = 09/03/15 Pct Recovery = 70% Analysis Date = 08/29/15 Pct Recovery = 70% Analysis Date = 08/29/15 Pct Recovery = 70% Analysis Date = 08/24/15 Pct Recovery = 70% Analysis Date = 08/24/15 Pct Recovery = 70% Analysis Date = 08/19/15 Pct Recovery = 70% Analysis Date = 08/19/15 Pct Recovery = 70% Analysis Date = 08/15/15 Pct Recovery = 70% Analysis Date = 08/15/15 Pct Recovery = 70% Analysis Date = 08/10/15 Pct Recovery = 70% Analysis Date = 08/10/15 Pct Recovery = 70% Analysis Date = 08/05/15 Pct Recovery = 70% Analysis Date = 08/05/15 Pct Recovery = 70% Analysis Date = 07/31/15 Pct Recovery = 70% Analysis Date = 07/31/15 Pct Recovery = 70% Analysis Date = 07/26/15 Pct Recovery = 70% Analysis Date = 07/26/15 Pct Recovery = 70% Analysis Date = 07/22/15 Pct Recovery = 70% Analysis Date = 07/22/15 Pct Recovery = 70% Analysis Date = 07/17/15 Pct Recovery = 70% Analysis Date = 07/17/15 Pct Recovery = 70% Analysis Date = 07/12/15 Pct Recovery = 70% Analysis Date = 07/12/15 Pct Recovery = 70% Analysis Date = 07/07/15 Pct Recovery = 70% Analysis Date = 07/07/15 Pct Recovery = 70% Analysis Date = 07/02/15 Pct Recovery = 70% Analysis Date = 07/02/15 Pct Recovery = 70% Analysis Date = 06/28/15 Pct Recovery = 70% Analysis Date = 06/28/15 Pct Recovery = 70% Analysis Date = 06/23/15 Pct Recovery = 70% Analysis Date = 06/23/15 Pct Recovery = 70% Analysis Date = 06/18/15 Pct Recovery = 70% Analysis Date = 06/18/15 Pct Recovery = 70% Analysis Date = 06/13/15 Pct Recovery = 70% Analysis Date = 06/13/15 Pct Recovery = 70% Analysis Date = 06/08/15 Pct Recovery = 70% Analysis Date = 06/08/15 Pct Recovery = 70% Analysis Date = 06/04/15 Pct Recovery = 70% Analysis Date = 06/04/15 Pct Recovery = 70% Analysis Date = 05/30/15 Pct Recovery = 70% Analysis Date = 05/30/15 Pct Recovery = 70% Analysis Date = 05/25/15 Pct Recovery = 70% Analysis Date = 05/25/15 Pct Recovery = 70% Analysis Date = 05/20/15 Pct Recovery = 70% Analysis Date = 05/20/15 Pct Recovery = 70% Analysis Date = 05/15/15 Pct Recovery = 70% Analysis Date = 05/15/15 Pct Recovery = 70% Analysis Date = 05/11/15 Pct Recovery = 70% Analysis Date = 05/11/15 Pct Recovery = 70% Analysis Date = 05/06/15 Pct Recovery = 70% Analysis Date = 05/06/15 Pct Recovery = 70% Analysis Date = 05/01/15 Pct Recovery = 70% Analysis Date = 05/01/15 Pct Recovery = 70% Analysis Date = 04/26/15 Pct Recovery = 70% Analysis Date = 04/26/15 Pct Recovery = 70% Analysis Date = 04/21/15 Pct Recovery = 70% Analysis Date = 04/21/15 Pct Recovery = 70% Analysis Date = 04/17/15 Pct Recovery = 70% Analysis Date = 04/17/15 Pct Recovery = 70% Analysis Date = 04/12/15 Pct Recovery = 69% Analysis Date = 04/12/15 Pct Recovery = 69% Analysis Date = 04/07/15 Pct Recovery = 69% Analysis Date = 04/07/15 Pct Recovery = 69% Analysis Date = 04/02/15 Pct Recovery = 69% Analysis Date = 04/02/15 Pct Recovery = 69% Analysis Date = 03/28/15 Pct Recovery = 69% Analysis Date = 03/28/15 Pct Recovery = 69% Analysis Date = 03/24/15 Pct Recovery = 69% Analysis Date = 03/24/15 Pct Recovery = 69% Analysis Date = 03/19/15 Pct Recovery = 69% Analysis Date = 03/19/15 Pct Recovery = 69% Analysis Date = 03/14/15 Pct Recovery = 69% Analysis Date = 03/14/15 Pct Recovery = 69% Analysis Date = 03/09/15 Pct Recovery = 69% Analysis Date = 03/09/15 Pct Recovery = 69% Analysis Date = 03/04/15 Pct Recovery = 69% Analysis Date = 03/04/15 Pct Recovery = 69% Analysis Date = 02/28/15 Pct Recovery = 69% Analysis Date = 02/28/15 Pct Recovery = 69% Analysis Date = 02/23/15 Pct Recovery = 69% Analysis Date = 02/23/15 Pct Recovery = 69% Analysis Date = 02/18/15 Pct Recovery = 69% Analysis Date = 02/18/15 Pct Recovery = 69% Analysis Date = 02/13/15 Pct Recovery = 69% Analysis Date = 02/13/15 Pct Recovery = 69% Analysis Date = 02/08/15 Pct Recovery = 69% Analysis Date = 02/08/15 Pct Recovery = 69% Analysis Date = 02/04/15 Pct Recovery = 69% Analysis Date = 02/04/15 Pct Recovery = 69% Analysis Date = 01/30/15 Pct Recovery = 69% Analysis Date = 01/30/15 Pct Recovery = 69% Analysis Date = 01/25/15 Pct Recovery = 69% Analysis Date = 01/25/15 Pct Recovery = 69% Analysis Date = 01/20/15 Pct Recovery = 69% Analysis Date = 01/20/15 Pct Recovery = 69% Analysis Date = 01/15/15 Pct Recovery = 69% Analysis Date = 01/15/15 Pct Recovery = 69% Analysis Date = 01/11/15 Pct Recovery = 69% Analysis Date = 01/11/15 Pct Recovery = 69% Analysis Date = 01/06/15 Pct Recovery = 69% Analysis Date = 01/06/15 Pct Recovery = 69% Analysis Date = 01/01/15 Pct Recovery = 69% Analysis Date = 01/01/15 Pct Recovery = 69% Analysis Date = 12/27/14 Pct Recovery = 69% Analysis Date = 12/27/14 Pct Recovery = 69% Analysis Date = 12/22/14 Pct Recovery = 69% Analysis Date = 12/22/14 Pct Recovery = 69% Analysis Date = 12/18/14 Pct Recovery = 69% Analysis Date = 12/18/14 Pct Recovery = 69% Analysis Date = 12/13/14 Pct Recovery = 69% Analysis Date = 12/13/14 Pct Recovery = 69% Analysis Date = 12/08/14 Pct Recovery = 69% Analysis Date = 12/08/14 Pct Recovery = 69% Analysis Date = 12/03/14 Pct Recovery = 69% Analysis Date = 12/03/14 Pct Recovery = 69% Analysis Date = 11/28/14 Pct Recovery = 69% Analysis Date = 11/28/14 Pct Recovery = 69% Analysis Date = 11/24/14 Pct Recovery = 69% Analysis Date = 11/24/14 Pct Recovery = 69% Analysis Date = 11/19/14 Pct Recovery = 69% Analysis Date = 11/19/14 Pct Recovery = 69% Analysis Date = 11/14/14 Pct Recovery = 69% Analysis Date = 11/14/14 Pct Recovery = 69% Analysis Date = 11/09/14 Pct Recovery = 69% Analysis Date = 11/09/14 Pct Recovery = 69% Analysis Date = 11/04/14 Pct Recovery = 69% Analysis Date = 11/04/14 Pct Recovery = 69% Analysis Date = 10/31/14 Pct Recovery = 69% Analysis Date = 10/31/14 Pct Recovery = 69% Analysis Date = 10/26/14 Pct Recovery = 69% Analysis Date = 10/26/14 Pct Recovery = 69% Analysis Date = 10/21/14 Pct Recovery = 69% Analysis Date = 10/21/14 Pct Recovery = 69% Analysis Date = 10/16/14 Pct Recovery = 69% Analysis Date = 10/16/14 Pct Recovery = 69% Analysis Date = 10/11/14 Pct Recovery = 69% Analysis Date = 10/11/14 Pct Recovery = 69% Analysis Date = 10/07/14 Pct Recovery = 69% Analysis Date = 10/07/14 Pct Recovery = 69% Analysis Date = 10/02/14 Pct Recovery = 69% Analysis Date = 10/02/14 Pct Recovery = 69% Analysis Date = 09/27/14 Pct Recovery = 69% Analysis Date = 09/27/14 Pct Recovery = 69% Analysis Date = 09/22/14 Pct Recovery = 69% Analysis Date = 09/22/14 Pct Recovery = 69% Analysis Date = 09/17/14 Pct Recovery = 69% Analysis Date = 09/17/14 Pct Recovery = 69% Analysis Date = 09/13/14 Pct Recovery = 69% Analysis Date = 09/13/14 Pct Recovery = 69% Analysis Date = 09/08/14 Pct Recovery = 69% Analysis Date = 09/08/14 Pct Recovery = 69% Analysis Date = 09/03/14 Pct Recovery = 69% Analysis Date = 09/03/14 Pct Recovery = 69% Analysis Date = 08/29/14 Pct Recovery = 68% Analysis Date = 08/29/14 Pct Recovery = 68% Analysis Date = 08/24/14 Pct Recovery = 68% Analysis Date = 08/24/14 Pct Recovery = 68% Analysis Date = 08/20/14 Pct Recovery = 68% Analysis Date = 08/20/14 Pct Recovery = 68% Analysis Date = 08/15/14 Pct Recovery = 68% Analysis Date = 08/15/14 Pct Recovery = 68% Analysis Date = 08/10/14 Pct Recovery = 68% Analysis Date = 08/10/14 Pct Recovery = 68% Analysis Date = 08/05/14 Pct Recovery = 68% Analysis Date = 08/05/14 Pct Recovery = 68% Analysis Date = 07/31/14 Pct Recovery = 68% Analysis Date = 07/31/14 Pct Recovery = 68% Analysis Date = 07/27/14 Pct Recovery = 68% Analysis Date = 07/27/14 Pct Recovery = 68% Analysis Date = 07/22/14 Pct Recovery = 68% Analysis Date = 07/22/14 Pct Recovery = 68% Analysis Date = 07/17/14 Pct Recovery = 68% Analysis Date = 07/17/14 Pct Recovery = 68% Analysis Date = 07/12/14 Pct Recovery = 68% Analysis Date = 07/12/14 Pct Recovery = 68% Analysis Date = 07/07/14 Pct Recovery = 68% Analysis Date = 07/07/14 Pct Recovery = 68% Analysis Date = 07/03/14 Pct Recovery = 68% Analysis Date = 07/03/14 Pct Recovery = 68% Analysis Date = 06/28/14 Pct Recovery = 68% Analysis Date = 06/28/14 Pct Recovery = 68% Analysis Date = 06/23/14 Pct Recovery = 68% Analysis Date = 06/23/14 Pct Recovery = 68% Analysis Date = 06/18/14 Pct Recovery = 68% Analysis Date = 06/18/14 Pct Recovery = 68% Analysis Date = 06/13/14 Pct Recovery = 68% Analysis Date = 06/13/14 Pct Recovery = 68% Analysis Date = 06/09/14 Pct Recovery = 68% Analysis Date = 06/09/14 Pct Recovery = 68% Analysis Date = 06/04/14 Pct Recovery = 68% Analysis Date = 06/04/14 Pct Recovery = 68% Analysis Date = 05/30/14 Pct Recovery = 68% Analysis Date = 05/30/14 Pct Recovery = 68% Analysis Date = 05/25/14 Pct Recovery = 68% Analysis Date = 05/25/14 Pct Recovery = 68% Analysis Date = 05/21/14 Pct Recovery = 68% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
OXYCODONE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 47 77% 17% 75% 14%
Total 47 77% 17% 75% 14%

Sample Statistics
OXYCODONE

Characteristic N % % Basis
Plotted 47 94% Spiked
Estimated Values 7 14% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 2 4% Spiked
Spiked 50 .  
False Negatives 1 2% 1 out of 50
Not Spiked 65 .  
False Positives 0 0% 0 out of 65

BQS OBSP Determination:
PAROXETINE
METHOD: 2440 , TESTIDCODE: 67527LCM56
Open Data Set

Analysis Date = 01/17/16 SpikeMix = ERA 0406-15-09: 80 µl & ERA 0406-15-07A: 80 µl Pct Recovery = 67% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 80 µl & Abs 051315: 80 µl Pct Recovery = 82% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 80 µl & ERA 0406-15-08: 80 µl Pct Recovery = 51% Analysis Date = 11/04/15 SpikeMix = Abs 052215: 80 µl & Abs 050115: 80 µl Pct Recovery = 42% Analysis Date = 09/24/16 SpikeMix = Crescent EN160610015: 80 µl & Abs 061416: 80 µl Pct Recovery = 49% Analysis Date = 09/24/16 SpikeMix = Abs 061416: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 55% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 59% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 59% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 51% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 61% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-04: 15 µl & Abs 041814: 15 µl Pct Recovery = 41% Analysis Date = 12/06/14 SpikeMix = ERA 0318-14-02: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 38% Analysis Date = 10/25/14 SpikeMix = Abs 041614: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 60% Analysis Date = 10/11/14 SpikeMix = ERA 0318-14-02: 60 µl & ERA 0319-14-04: 60 µl Pct Recovery = 62% Analysis Date = 08/28/14 SpikeMix = ERA 0319-14-04: 60 µl & ERA 0319-14-05: 60 µl Pct Recovery = 48% Analysis Date = 05/07/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 25% Analysis Date = 03/11/15 SpikeMix = ERA 0318-14-02: 15 µl & Abs 041714: 15 µl Pct Recovery = 38% Analysis Date = 01/16/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 35% Analysis Date = 12/06/14 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 26% Analysis Date = 08/21/14 SpikeMix = ERA 0318-14-02: 60 µl & Abs 041714: 60 µl Pct Recovery = 19% Analysis Date = 07/12/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 45% Analysis Date = 06/11/14 SpikeMix = Abs 041614: 60 µl & Abs 041714: 60 µl Pct Recovery = 27% Analysis Date = 05/21/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 52% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-07A: 40 µl & Abs 051315: 40 µl Pct Recovery = 53% Analysis Date = 11/04/15 SpikeMix = ERA 0406-15-07A: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 56% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 56% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 54% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 33% Analysis Date = 02/23/16 SpikeMix = Abs 052215: 40 µl & Abs 050115: 40 µl Pct Recovery = 45% Analysis Date = 07/31/15 SpikeMix = ERA 0406-15-09: 40 µl & Abs 050115: 40 µl Pct Recovery = 48% Analysis Date = 07/30/15 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 42% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 32% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 47% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 39% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 34% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 21% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 36% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 38% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 51% Analysis Date = 04/30/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 53% Analysis Date = 02/10/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 17% Analysis Date = 12/07/14 SpikeMix = ERA 0318-14-02: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 59% Analysis Date = 10/11/14 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 43% Analysis Date = 11/04/14 SpikeMix = Abs 041714: 8 µl & ERA 0319-14-05: 8 µl Pct Recovery = 15% Analysis Date = 09/12/14 SpikeMix = Abs 041614: 30 µl & ERA 0319-14-04: 30 µl Pct Recovery = 41% Analysis Date = 08/16/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 43% Analysis Date = 07/13/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 22% Analysis Date = 04/23/14 SpikeMix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.2: 20 µl Pct Recovery = 71% Analysis Date = 06/28/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 53% Analysis Date = 05/17/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 58% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 47% Analysis Date = 04/27/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 70% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 67% Analysis Date = 11/24/15 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 47% Analysis Date = 09/15/15 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 46% Analysis Date = 11/25/15 SpikeMix = Abs 050115: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 25% Analysis Date = 11/24/15 SpikeMix = ERA 0406-15-09: 20 µl & Abs 050115: 20 µl Pct Recovery = 41% Analysis Date = 07/09/15 SpikeMix = Abs 050115: 20 µl & Abs 052215: 20 µl Pct Recovery = 41% Analysis Date = 06/09/15 SpikeMix = Abs 051315: 20 µl & Abs 050115: 20 µl Pct Recovery = 41% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 58% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 57% Analysis Date = 11/18/16 SpikeMix = ERA 04281604: 80 µl & ERA 04281603: 80 µl Pct Recovery = 56% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & ERA 04281604: 80 µl Pct Recovery = 44% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 53% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 61% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 81% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 95% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 66% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 70% Analysis Date = 01/04/17 Pct Recovery = 60% Analysis Date = 12/31/16 Pct Recovery = 60% Analysis Date = 12/31/16 Pct Recovery = 60% Analysis Date = 12/26/16 Pct Recovery = 60% Analysis Date = 12/26/16 Pct Recovery = 60% Analysis Date = 12/21/16 Pct Recovery = 59% Analysis Date = 12/21/16 Pct Recovery = 59% Analysis Date = 12/16/16 Pct Recovery = 59% Analysis Date = 12/16/16 Pct Recovery = 59% Analysis Date = 12/11/16 Pct Recovery = 59% Analysis Date = 12/11/16 Pct Recovery = 59% Analysis Date = 12/06/16 Pct Recovery = 58% Analysis Date = 12/06/16 Pct Recovery = 58% Analysis Date = 12/01/16 Pct Recovery = 58% Analysis Date = 12/01/16 Pct Recovery = 58% Analysis Date = 11/26/16 Pct Recovery = 58% Analysis Date = 11/26/16 Pct Recovery = 58% Analysis Date = 11/21/16 Pct Recovery = 58% Analysis Date = 11/21/16 Pct Recovery = 58% Analysis Date = 11/16/16 Pct Recovery = 57% Analysis Date = 11/16/16 Pct Recovery = 57% Analysis Date = 11/11/16 Pct Recovery = 57% Analysis Date = 11/11/16 Pct Recovery = 57% Analysis Date = 11/06/16 Pct Recovery = 57% Analysis Date = 11/06/16 Pct Recovery = 57% Analysis Date = 11/01/16 Pct Recovery = 56% Analysis Date = 11/01/16 Pct Recovery = 56% Analysis Date = 10/27/16 Pct Recovery = 56% Analysis Date = 10/27/16 Pct Recovery = 56% Analysis Date = 10/22/16 Pct Recovery = 56% Analysis Date = 10/22/16 Pct Recovery = 56% Analysis Date = 10/17/16 Pct Recovery = 56% Analysis Date = 10/17/16 Pct Recovery = 56% Analysis Date = 10/13/16 Pct Recovery = 55% Analysis Date = 10/13/16 Pct Recovery = 55% Analysis Date = 10/08/16 Pct Recovery = 55% Analysis Date = 10/08/16 Pct Recovery = 55% Analysis Date = 10/03/16 Pct Recovery = 55% Analysis Date = 10/03/16 Pct Recovery = 55% Analysis Date = 09/28/16 Pct Recovery = 55% Analysis Date = 09/28/16 Pct Recovery = 55% Analysis Date = 09/23/16 Pct Recovery = 54% Analysis Date = 09/23/16 Pct Recovery = 54% Analysis Date = 09/18/16 Pct Recovery = 54% Analysis Date = 09/18/16 Pct Recovery = 54% Analysis Date = 09/13/16 Pct Recovery = 54% Analysis Date = 09/13/16 Pct Recovery = 54% Analysis Date = 09/08/16 Pct Recovery = 54% Analysis Date = 09/08/16 Pct Recovery = 54% Analysis Date = 09/03/16 Pct Recovery = 54% Analysis Date = 09/03/16 Pct Recovery = 54% Analysis Date = 08/29/16 Pct Recovery = 53% Analysis Date = 08/29/16 Pct Recovery = 53% Analysis Date = 08/24/16 Pct Recovery = 53% Analysis Date = 08/24/16 Pct Recovery = 53% Analysis Date = 08/19/16 Pct Recovery = 53% Analysis Date = 08/19/16 Pct Recovery = 53% Analysis Date = 08/14/16 Pct Recovery = 53% Analysis Date = 08/14/16 Pct Recovery = 53% Analysis Date = 08/09/16 Pct Recovery = 53% Analysis Date = 08/09/16 Pct Recovery = 53% Analysis Date = 08/04/16 Pct Recovery = 52% Analysis Date = 08/04/16 Pct Recovery = 52% Analysis Date = 07/30/16 Pct Recovery = 52% Analysis Date = 07/30/16 Pct Recovery = 52% Analysis Date = 07/25/16 Pct Recovery = 52% Analysis Date = 07/25/16 Pct Recovery = 52% Analysis Date = 07/21/16 Pct Recovery = 52% Analysis Date = 07/21/16 Pct Recovery = 52% Analysis Date = 07/16/16 Pct Recovery = 52% Analysis Date = 07/16/16 Pct Recovery = 52% Analysis Date = 07/11/16 Pct Recovery = 52% Analysis Date = 07/11/16 Pct Recovery = 52% Analysis Date = 07/06/16 Pct Recovery = 52% Analysis Date = 07/06/16 Pct Recovery = 52% Analysis Date = 07/01/16 Pct Recovery = 52% Analysis Date = 07/01/16 Pct Recovery = 52% Analysis Date = 06/26/16 Pct Recovery = 51% Analysis Date = 06/26/16 Pct Recovery = 51% Analysis Date = 06/21/16 Pct Recovery = 51% Analysis Date = 06/21/16 Pct Recovery = 51% Analysis Date = 06/16/16 Pct Recovery = 51% Analysis Date = 06/16/16 Pct Recovery = 51% Analysis Date = 06/11/16 Pct Recovery = 51% Analysis Date = 06/11/16 Pct Recovery = 51% Analysis Date = 06/06/16 Pct Recovery = 51% Analysis Date = 06/06/16 Pct Recovery = 51% Analysis Date = 06/01/16 Pct Recovery = 51% Analysis Date = 06/01/16 Pct Recovery = 51% Analysis Date = 05/27/16 Pct Recovery = 51% Analysis Date = 05/27/16 Pct Recovery = 51% Analysis Date = 05/22/16 Pct Recovery = 51% Analysis Date = 05/22/16 Pct Recovery = 51% Analysis Date = 05/17/16 Pct Recovery = 50% Analysis Date = 05/17/16 Pct Recovery = 50% Analysis Date = 05/12/16 Pct Recovery = 50% Analysis Date = 05/12/16 Pct Recovery = 50% Analysis Date = 05/07/16 Pct Recovery = 50% Analysis Date = 05/07/16 Pct Recovery = 50% Analysis Date = 05/02/16 Pct Recovery = 50% Analysis Date = 05/02/16 Pct Recovery = 50% Analysis Date = 04/28/16 Pct Recovery = 50% Analysis Date = 04/28/16 Pct Recovery = 50% Analysis Date = 04/23/16 Pct Recovery = 50% Analysis Date = 04/23/16 Pct Recovery = 50% Analysis Date = 04/18/16 Pct Recovery = 50% Analysis Date = 04/18/16 Pct Recovery = 50% Analysis Date = 04/13/16 Pct Recovery = 50% Analysis Date = 04/13/16 Pct Recovery = 50% Analysis Date = 04/08/16 Pct Recovery = 50% Analysis Date = 04/08/16 Pct Recovery = 50% Analysis Date = 04/03/16 Pct Recovery = 50% Analysis Date = 04/03/16 Pct Recovery = 50% Analysis Date = 03/29/16 Pct Recovery = 50% Analysis Date = 03/29/16 Pct Recovery = 50% Analysis Date = 03/24/16 Pct Recovery = 50% Analysis Date = 03/24/16 Pct Recovery = 50% Analysis Date = 03/19/16 Pct Recovery = 50% Analysis Date = 03/19/16 Pct Recovery = 50% Analysis Date = 03/14/16 Pct Recovery = 50% Analysis Date = 03/14/16 Pct Recovery = 50% Analysis Date = 03/09/16 Pct Recovery = 50% Analysis Date = 03/09/16 Pct Recovery = 50% Analysis Date = 03/04/16 Pct Recovery = 50% Analysis Date = 03/04/16 Pct Recovery = 50% Analysis Date = 02/28/16 Pct Recovery = 50% Analysis Date = 02/28/16 Pct Recovery = 50% Analysis Date = 02/23/16 Pct Recovery = 50% Analysis Date = 02/23/16 Pct Recovery = 50% Analysis Date = 02/18/16 Pct Recovery = 50% Analysis Date = 02/18/16 Pct Recovery = 50% Analysis Date = 02/13/16 Pct Recovery = 50% Analysis Date = 02/13/16 Pct Recovery = 50% Analysis Date = 02/09/16 Pct Recovery = 50% Analysis Date = 02/09/16 Pct Recovery = 50% Analysis Date = 02/04/16 Pct Recovery = 50% Analysis Date = 02/04/16 Pct Recovery = 50% Analysis Date = 01/30/16 Pct Recovery = 50% Analysis Date = 01/30/16 Pct Recovery = 50% Analysis Date = 01/25/16 Pct Recovery = 50% Analysis Date = 01/25/16 Pct Recovery = 50% Analysis Date = 01/20/16 Pct Recovery = 50% Analysis Date = 01/20/16 Pct Recovery = 50% Analysis Date = 01/15/16 Pct Recovery = 50% Analysis Date = 01/15/16 Pct Recovery = 50% Analysis Date = 01/10/16 Pct Recovery = 50% Analysis Date = 01/10/16 Pct Recovery = 50% Analysis Date = 01/05/16 Pct Recovery = 50% Analysis Date = 01/05/16 Pct Recovery = 50% Analysis Date = 12/31/15 Pct Recovery = 50% Analysis Date = 12/31/15 Pct Recovery = 50% Analysis Date = 12/26/15 Pct Recovery = 50% Analysis Date = 12/26/15 Pct Recovery = 50% Analysis Date = 12/21/15 Pct Recovery = 50% Analysis Date = 12/21/15 Pct Recovery = 50% Analysis Date = 12/16/15 Pct Recovery = 49% Analysis Date = 12/16/15 Pct Recovery = 49% Analysis Date = 12/11/15 Pct Recovery = 49% Analysis Date = 12/11/15 Pct Recovery = 49% Analysis Date = 12/06/15 Pct Recovery = 49% Analysis Date = 12/06/15 Pct Recovery = 49% Analysis Date = 12/01/15 Pct Recovery = 49% Analysis Date = 12/01/15 Pct Recovery = 49% Analysis Date = 11/26/15 Pct Recovery = 49% Analysis Date = 11/26/15 Pct Recovery = 49% Analysis Date = 11/21/15 Pct Recovery = 49% Analysis Date = 11/21/15 Pct Recovery = 49% Analysis Date = 11/17/15 Pct Recovery = 49% Analysis Date = 11/17/15 Pct Recovery = 49% Analysis Date = 11/12/15 Pct Recovery = 49% Analysis Date = 11/12/15 Pct Recovery = 49% Analysis Date = 11/07/15 Pct Recovery = 48% Analysis Date = 11/07/15 Pct Recovery = 48% Analysis Date = 11/02/15 Pct Recovery = 48% Analysis Date = 11/02/15 Pct Recovery = 48% Analysis Date = 10/28/15 Pct Recovery = 48% Analysis Date = 10/28/15 Pct Recovery = 48% Analysis Date = 10/23/15 Pct Recovery = 48% Analysis Date = 10/23/15 Pct Recovery = 48% Analysis Date = 10/18/15 Pct Recovery = 48% Analysis Date = 10/18/15 Pct Recovery = 48% Analysis Date = 10/13/15 Pct Recovery = 47% Analysis Date = 10/13/15 Pct Recovery = 47% Analysis Date = 10/08/15 Pct Recovery = 47% Analysis Date = 10/08/15 Pct Recovery = 47% Analysis Date = 10/03/15 Pct Recovery = 47% Analysis Date = 10/03/15 Pct Recovery = 47% Analysis Date = 09/28/15 Pct Recovery = 47% Analysis Date = 09/28/15 Pct Recovery = 47% Analysis Date = 09/23/15 Pct Recovery = 47% Analysis Date = 09/23/15 Pct Recovery = 47% Analysis Date = 09/18/15 Pct Recovery = 46% Analysis Date = 09/18/15 Pct Recovery = 46% Analysis Date = 09/13/15 Pct Recovery = 46% Analysis Date = 09/13/15 Pct Recovery = 46% Analysis Date = 09/08/15 Pct Recovery = 46% Analysis Date = 09/08/15 Pct Recovery = 46% Analysis Date = 09/03/15 Pct Recovery = 46% Analysis Date = 09/03/15 Pct Recovery = 46% Analysis Date = 08/29/15 Pct Recovery = 46% Analysis Date = 08/29/15 Pct Recovery = 46% Analysis Date = 08/25/15 Pct Recovery = 45% Analysis Date = 08/25/15 Pct Recovery = 45% Analysis Date = 08/20/15 Pct Recovery = 45% Analysis Date = 08/20/15 Pct Recovery = 45% Analysis Date = 08/15/15 Pct Recovery = 45% Analysis Date = 08/15/15 Pct Recovery = 45% Analysis Date = 08/10/15 Pct Recovery = 45% Analysis Date = 08/10/15 Pct Recovery = 45% Analysis Date = 08/05/15 Pct Recovery = 45% Analysis Date = 08/05/15 Pct Recovery = 45% Analysis Date = 07/31/15 Pct Recovery = 45% Analysis Date = 07/31/15 Pct Recovery = 45% Analysis Date = 07/26/15 Pct Recovery = 44% Analysis Date = 07/26/15 Pct Recovery = 44% Analysis Date = 07/21/15 Pct Recovery = 44% Analysis Date = 07/21/15 Pct Recovery = 44% Analysis Date = 07/16/15 Pct Recovery = 44% Analysis Date = 07/16/15 Pct Recovery = 44% Analysis Date = 07/11/15 Pct Recovery = 44% Analysis Date = 07/11/15 Pct Recovery = 44% Analysis Date = 07/06/15 Pct Recovery = 44% Analysis Date = 07/06/15 Pct Recovery = 44% Analysis Date = 07/01/15 Pct Recovery = 44% Analysis Date = 07/01/15 Pct Recovery = 44% Analysis Date = 06/26/15 Pct Recovery = 44% Analysis Date = 06/26/15 Pct Recovery = 44% Analysis Date = 06/21/15 Pct Recovery = 44% Analysis Date = 06/21/15 Pct Recovery = 44% Analysis Date = 06/16/15 Pct Recovery = 44% Analysis Date = 06/16/15 Pct Recovery = 44% Analysis Date = 06/11/15 Pct Recovery = 43% Analysis Date = 06/11/15 Pct Recovery = 43% Analysis Date = 06/07/15 Pct Recovery = 43% Analysis Date = 06/07/15 Pct Recovery = 43% Analysis Date = 06/02/15 Pct Recovery = 43% Analysis Date = 06/02/15 Pct Recovery = 43% Analysis Date = 05/28/15 Pct Recovery = 43% Analysis Date = 05/28/15 Pct Recovery = 43% Analysis Date = 05/23/15 Pct Recovery = 43% Analysis Date = 05/23/15 Pct Recovery = 43% Analysis Date = 05/18/15 Pct Recovery = 43% Analysis Date = 05/18/15 Pct Recovery = 43% Analysis Date = 05/13/15 Pct Recovery = 43% Analysis Date = 05/13/15 Pct Recovery = 43% Analysis Date = 05/08/15 Pct Recovery = 43% Analysis Date = 05/08/15 Pct Recovery = 43% Analysis Date = 05/03/15 Pct Recovery = 43% Analysis Date = 05/03/15 Pct Recovery = 43% Analysis Date = 04/28/15 Pct Recovery = 42% Analysis Date = 04/28/15 Pct Recovery = 42% Analysis Date = 04/23/15 Pct Recovery = 42% Analysis Date = 04/23/15 Pct Recovery = 42% Analysis Date = 04/18/15 Pct Recovery = 42% Analysis Date = 04/18/15 Pct Recovery = 42% Analysis Date = 04/13/15 Pct Recovery = 42% Analysis Date = 04/13/15 Pct Recovery = 42% Analysis Date = 04/08/15 Pct Recovery = 42% Analysis Date = 04/08/15 Pct Recovery = 42% Analysis Date = 04/03/15 Pct Recovery = 42% Analysis Date = 04/03/15 Pct Recovery = 42% Analysis Date = 03/29/15 Pct Recovery = 42% Analysis Date = 03/29/15 Pct Recovery = 42% Analysis Date = 03/24/15 Pct Recovery = 42% Analysis Date = 03/24/15 Pct Recovery = 42% Analysis Date = 03/19/15 Pct Recovery = 42% Analysis Date = 03/19/15 Pct Recovery = 42% Analysis Date = 03/15/15 Pct Recovery = 42% Analysis Date = 03/15/15 Pct Recovery = 42% Analysis Date = 03/10/15 Pct Recovery = 42% Analysis Date = 03/10/15 Pct Recovery = 42% Analysis Date = 03/05/15 Pct Recovery = 42% Analysis Date = 03/05/15 Pct Recovery = 42% Analysis Date = 02/28/15 Pct Recovery = 42% Analysis Date = 02/28/15 Pct Recovery = 42% Analysis Date = 02/23/15 Pct Recovery = 42% Analysis Date = 02/23/15 Pct Recovery = 42% Analysis Date = 02/18/15 Pct Recovery = 42% Analysis Date = 02/18/15 Pct Recovery = 42% Analysis Date = 02/13/15 Pct Recovery = 42% Analysis Date = 02/13/15 Pct Recovery = 42% Analysis Date = 02/08/15 Pct Recovery = 42% Analysis Date = 02/08/15 Pct Recovery = 42% Analysis Date = 02/03/15 Pct Recovery = 42% Analysis Date = 02/03/15 Pct Recovery = 42% Analysis Date = 01/29/15 Pct Recovery = 42% Analysis Date = 01/29/15 Pct Recovery = 42% Analysis Date = 01/24/15 Pct Recovery = 42% Analysis Date = 01/24/15 Pct Recovery = 42% Analysis Date = 01/19/15 Pct Recovery = 42% Analysis Date = 01/19/15 Pct Recovery = 42% Analysis Date = 01/14/15 Pct Recovery = 42% Analysis Date = 01/14/15 Pct Recovery = 42% Analysis Date = 01/09/15 Pct Recovery = 42% Analysis Date = 01/09/15 Pct Recovery = 42% Analysis Date = 01/04/15 Pct Recovery = 42% Analysis Date = 01/04/15 Pct Recovery = 42% Analysis Date = 12/30/14 Pct Recovery = 42% Analysis Date = 12/30/14 Pct Recovery = 42% Analysis Date = 12/25/14 Pct Recovery = 42% Analysis Date = 12/25/14 Pct Recovery = 42% Analysis Date = 12/21/14 Pct Recovery = 42% Analysis Date = 12/21/14 Pct Recovery = 42% Analysis Date = 12/16/14 Pct Recovery = 42% Analysis Date = 12/16/14 Pct Recovery = 42% Analysis Date = 12/11/14 Pct Recovery = 42% Analysis Date = 12/11/14 Pct Recovery = 42% Analysis Date = 12/06/14 Pct Recovery = 42% Analysis Date = 12/06/14 Pct Recovery = 42% Analysis Date = 12/01/14 Pct Recovery = 42% Analysis Date = 12/01/14 Pct Recovery = 42% Analysis Date = 11/26/14 Pct Recovery = 42% Analysis Date = 11/26/14 Pct Recovery = 42% Analysis Date = 11/21/14 Pct Recovery = 42% Analysis Date = 11/21/14 Pct Recovery = 42% Analysis Date = 11/16/14 Pct Recovery = 42% Analysis Date = 11/16/14 Pct Recovery = 42% Analysis Date = 11/11/14 Pct Recovery = 42% Analysis Date = 11/11/14 Pct Recovery = 42% Analysis Date = 11/06/14 Pct Recovery = 42% Analysis Date = 11/06/14 Pct Recovery = 42% Analysis Date = 11/01/14 Pct Recovery = 42% Analysis Date = 11/01/14 Pct Recovery = 42% Analysis Date = 10/27/14 Pct Recovery = 42% Analysis Date = 10/27/14 Pct Recovery = 42% Analysis Date = 10/22/14 Pct Recovery = 42% Analysis Date = 10/22/14 Pct Recovery = 42% Analysis Date = 10/17/14 Pct Recovery = 42% Analysis Date = 10/17/14 Pct Recovery = 42% Analysis Date = 10/12/14 Pct Recovery = 42% Analysis Date = 10/12/14 Pct Recovery = 42% Analysis Date = 10/07/14 Pct Recovery = 42% Analysis Date = 10/07/14 Pct Recovery = 42% Analysis Date = 10/03/14 Pct Recovery = 43% Analysis Date = 10/03/14 Pct Recovery = 43% Analysis Date = 09/28/14 Pct Recovery = 43% Analysis Date = 09/28/14 Pct Recovery = 43% Analysis Date = 09/23/14 Pct Recovery = 43% Analysis Date = 09/23/14 Pct Recovery = 43% Analysis Date = 09/18/14 Pct Recovery = 43% Analysis Date = 09/18/14 Pct Recovery = 43% Analysis Date = 09/13/14 Pct Recovery = 43% Analysis Date = 09/13/14 Pct Recovery = 43% Analysis Date = 09/08/14 Pct Recovery = 43% Analysis Date = 09/08/14 Pct Recovery = 43% Analysis Date = 09/03/14 Pct Recovery = 43% Analysis Date = 09/03/14 Pct Recovery = 43% Analysis Date = 08/29/14 Pct Recovery = 43% Analysis Date = 08/29/14 Pct Recovery = 43% Analysis Date = 08/24/14 Pct Recovery = 43% Analysis Date = 08/24/14 Pct Recovery = 43% Analysis Date = 08/19/14 Pct Recovery = 43% Analysis Date = 08/19/14 Pct Recovery = 43% Analysis Date = 08/14/14 Pct Recovery = 43% Analysis Date = 08/14/14 Pct Recovery = 43% Analysis Date = 08/09/14 Pct Recovery = 43% Analysis Date = 08/09/14 Pct Recovery = 43% Analysis Date = 08/04/14 Pct Recovery = 43% Analysis Date = 08/04/14 Pct Recovery = 43% Analysis Date = 07/30/14 Pct Recovery = 43% Analysis Date = 07/30/14 Pct Recovery = 43% Analysis Date = 07/25/14 Pct Recovery = 44% Analysis Date = 07/25/14 Pct Recovery = 44% Analysis Date = 07/20/14 Pct Recovery = 44% Analysis Date = 07/20/14 Pct Recovery = 44% Analysis Date = 07/15/14 Pct Recovery = 44% Analysis Date = 07/15/14 Pct Recovery = 44% Analysis Date = 07/11/14 Pct Recovery = 44% Analysis Date = 07/11/14 Pct Recovery = 44% Analysis Date = 07/06/14 Pct Recovery = 44% Analysis Date = 07/06/14 Pct Recovery = 44% Analysis Date = 07/01/14 Pct Recovery = 44% Analysis Date = 07/01/14 Pct Recovery = 44% Analysis Date = 06/26/14 Pct Recovery = 44% Analysis Date = 06/26/14 Pct Recovery = 44% Analysis Date = 06/21/14 Pct Recovery = 44% Analysis Date = 06/21/14 Pct Recovery = 44% Analysis Date = 06/16/14 Pct Recovery = 44% Analysis Date = 06/16/14 Pct Recovery = 44% Analysis Date = 06/11/14 Pct Recovery = 44% Analysis Date = 06/11/14 Pct Recovery = 44% Analysis Date = 06/06/14 Pct Recovery = 44% Analysis Date = 06/06/14 Pct Recovery = 44% Analysis Date = 06/01/14 Pct Recovery = 45% Analysis Date = 06/01/14 Pct Recovery = 45% Analysis Date = 05/27/14 Pct Recovery = 45% Analysis Date = 05/27/14 Pct Recovery = 45% Analysis Date = 05/22/14 Pct Recovery = 45% Analysis Date = 05/22/14 Pct Recovery = 45% Analysis Date = 05/17/14 Pct Recovery = 45% Analysis Date = 05/17/14 Pct Recovery = 45% Analysis Date = 05/12/14 Pct Recovery = 45% Analysis Date = 05/12/14 Pct Recovery = 45% Analysis Date = 05/07/14 Pct Recovery = 45% Analysis Date = 05/07/14 Pct Recovery = 45% Analysis Date = 05/02/14 Pct Recovery = 45% Analysis Date = 05/02/14 Pct Recovery = 45% Analysis Date = 04/27/14 Pct Recovery = 45% Analysis Date = 04/27/14 Pct Recovery = 45% Analysis Date = 04/23/14 Pct Recovery = 45% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
PAROXETINE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 10 64% 15% 60% 10%
>= Reporting Level 59 45% 14% 46% 13%
Total 69 48% 16% 48% 14%

Sample Statistics
PAROXETINE

Characteristic N % % Basis
Plotted 69 87% Spiked
Estimated Values 69 87% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 79 .  
False Negatives 10 13% 10 out of 79
Not Spiked 36 .  
False Positives 0 0% 0 out of 36

BQS OBSP Determination:
PENCICLOVIR
METHOD: 2440 , TESTIDCODE: 68021LCM56
Open Data Set

Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 39% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 36% Analysis Date = 11/05/15 SpikeMix = ERA 0406-15-08: 80 µl & Abs 052215: 80 µl Pct Recovery = 96% Analysis Date = 11/04/15 SpikeMix = Abs 052215: 80 µl & Abs 050115: 80 µl Pct Recovery = 87% Analysis Date = 01/17/16 SpikeMix = ERA 0406-15-09: 80 µl & ERA 0406-15-07A: 80 µl Pct Recovery = 73% Analysis Date = 11/24/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 64% Analysis Date = 10/01/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 67% Analysis Date = 09/24/16 SpikeMix = Crescent EN160610015: 80 µl & Abs 061416: 80 µl Pct Recovery = 74% Analysis Date = 09/24/16 SpikeMix = Abs 061416: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 72% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 136% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 127% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 133% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 128% Analysis Date = 11/18/16 SpikeMix = ERA 04281604: 80 µl & ERA 04281603: 80 µl Pct Recovery = 35% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & ERA 04281604: 80 µl Pct Recovery = 38% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 132% Analysis Date = 12/07/14 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 106% Analysis Date = 10/25/14 SpikeMix = Abs 041614: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 128% Analysis Date = 06/22/14 SpikeMix = Abs 041814: 60 µl & Abs 041614: 60 µl Pct Recovery = 123% Analysis Date = 06/11/14 SpikeMix = Abs 041614: 60 µl & Abs 041714: 60 µl Pct Recovery = 111% Analysis Date = 04/29/15 SpikeMix = ERA 0319-14-05: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 103% Analysis Date = 03/11/15 SpikeMix = ERA 0318-14-02: 15 µl & Abs 041714: 15 µl Pct Recovery = 93% Analysis Date = 02/06/15 SpikeMix = Abs 041814: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 76% Analysis Date = 12/06/14 SpikeMix = ERA 0318-14-02: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 69% Analysis Date = 10/11/14 SpikeMix = ERA 0318-14-02: 60 µl & ERA 0319-14-04: 60 µl Pct Recovery = 68% Analysis Date = 08/21/14 SpikeMix = ERA 0318-14-02: 60 µl & Abs 041714: 60 µl Pct Recovery = 64% Analysis Date = 07/26/14 SpikeMix = ERA 0319-14-05: 60 µl & ERA 0318-14-02: 60 µl Pct Recovery = 64% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-08: 40 µl & Abs 052215: 40 µl Pct Recovery = 105% Analysis Date = 02/23/16 SpikeMix = Abs 052215: 40 µl & Abs 050115: 40 µl Pct Recovery = 65% Analysis Date = 09/10/15 SpikeMix = Abs 052215: 40 µl & ERA 0406-15-07A: 40 µl Pct Recovery = 101% Analysis Date = 07/31/15 SpikeMix = Abs 051315: 40 µl & Abs 052215: 40 µl Pct Recovery = 108% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 92% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 71% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 79% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 85% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 56% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 66% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 63% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 65% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 49% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 50% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 43% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 34% Analysis Date = 04/30/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 139% Analysis Date = 02/10/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 127% Analysis Date = 10/24/14 SpikeMix = ERA 0319-14-05: 8 µl & Abs 041614: 8 µl Pct Recovery = 133% Analysis Date = 12/07/14 SpikeMix = ERA 0318-14-02: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 70% Analysis Date = 11/04/14 SpikeMix = Abs 041814: 8 µl & ERA 0318-14-02: 8 µl Pct Recovery = 71% Analysis Date = 09/12/14 SpikeMix = Abs 041614: 30 µl & ERA 0319-14-04: 30 µl Pct Recovery = 113% Analysis Date = 07/13/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 108% Analysis Date = 06/28/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 93% Analysis Date = 05/30/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 112% Analysis Date = 05/17/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 123% Analysis Date = 04/23/14 SpikeMix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.2: 20 µl Pct Recovery = 118% Analysis Date = 10/10/14 SpikeMix = Abs 041814: 30 µl & ERA 0318-14-02: 30 µl Pct Recovery = 59% Analysis Date = 08/30/14 SpikeMix = ERA 0318-14-02: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 54% Analysis Date = 07/20/14 SpikeMix = ERA 0318-14-02: 30 µl & Abs 041714: 30 µl Pct Recovery = 61% Analysis Date = 11/24/15 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 60% Analysis Date = 08/27/15 SpikeMix = Abs 052215: 20 µl & Abs 050115: 20 µl Pct Recovery = 74% Analysis Date = 07/09/15 SpikeMix = Abs 050115: 20 µl & Abs 052215: 20 µl Pct Recovery = 120% Analysis Date = 06/26/15 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 103% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-08: 20 µl & ERA 0406-15-09: 20 µl Pct Recovery = 56% Analysis Date = 11/24/15 SpikeMix = ERA 0406-15-09: 20 µl & Abs 050115: 20 µl Pct Recovery = 76% Analysis Date = 04/09/16 SpikeMix = Abs 051315: 10 µl & ERA 0406-15-09: 10 µl Pct Recovery = 142% Analysis Date = 12/16/16 Pct Recovery = 60% Analysis Date = 12/11/16 Pct Recovery = 61% Analysis Date = 12/11/16 Pct Recovery = 61% Analysis Date = 12/06/16 Pct Recovery = 62% Analysis Date = 12/06/16 Pct Recovery = 62% Analysis Date = 12/01/16 Pct Recovery = 62% Analysis Date = 12/01/16 Pct Recovery = 62% Analysis Date = 11/26/16 Pct Recovery = 63% Analysis Date = 11/26/16 Pct Recovery = 63% Analysis Date = 11/21/16 Pct Recovery = 63% Analysis Date = 11/21/16 Pct Recovery = 63% Analysis Date = 11/16/16 Pct Recovery = 64% Analysis Date = 11/16/16 Pct Recovery = 64% Analysis Date = 11/12/16 Pct Recovery = 65% Analysis Date = 11/12/16 Pct Recovery = 65% Analysis Date = 11/07/16 Pct Recovery = 65% Analysis Date = 11/07/16 Pct Recovery = 65% Analysis Date = 11/02/16 Pct Recovery = 66% Analysis Date = 11/02/16 Pct Recovery = 66% Analysis Date = 10/28/16 Pct Recovery = 66% Analysis Date = 10/28/16 Pct Recovery = 66% Analysis Date = 10/23/16 Pct Recovery = 67% Analysis Date = 10/23/16 Pct Recovery = 67% Analysis Date = 10/18/16 Pct Recovery = 67% Analysis Date = 10/18/16 Pct Recovery = 67% Analysis Date = 10/14/16 Pct Recovery = 68% Analysis Date = 10/14/16 Pct Recovery = 68% Analysis Date = 10/09/16 Pct Recovery = 68% Analysis Date = 10/09/16 Pct Recovery = 68% Analysis Date = 10/04/16 Pct Recovery = 69% Analysis Date = 10/04/16 Pct Recovery = 69% Analysis Date = 09/29/16 Pct Recovery = 69% Analysis Date = 09/29/16 Pct Recovery = 69% Analysis Date = 09/24/16 Pct Recovery = 70% Analysis Date = 09/24/16 Pct Recovery = 70% Analysis Date = 09/19/16 Pct Recovery = 70% Analysis Date = 09/19/16 Pct Recovery = 70% Analysis Date = 09/15/16 Pct Recovery = 71% Analysis Date = 09/15/16 Pct Recovery = 71% Analysis Date = 09/10/16 Pct Recovery = 71% Analysis Date = 09/10/16 Pct Recovery = 71% Analysis Date = 09/05/16 Pct Recovery = 72% Analysis Date = 09/05/16 Pct Recovery = 72% Analysis Date = 08/31/16 Pct Recovery = 72% Analysis Date = 08/31/16 Pct Recovery = 72% Analysis Date = 08/26/16 Pct Recovery = 72% Analysis Date = 08/26/16 Pct Recovery = 72% Analysis Date = 08/21/16 Pct Recovery = 73% Analysis Date = 08/21/16 Pct Recovery = 73% Analysis Date = 08/17/16 Pct Recovery = 73% Analysis Date = 08/17/16 Pct Recovery = 73% Analysis Date = 08/12/16 Pct Recovery = 74% Analysis Date = 08/12/16 Pct Recovery = 74% Analysis Date = 08/07/16 Pct Recovery = 74% Analysis Date = 08/07/16 Pct Recovery = 74% Analysis Date = 08/02/16 Pct Recovery = 74% Analysis Date = 08/02/16 Pct Recovery = 74% Analysis Date = 07/28/16 Pct Recovery = 75% Analysis Date = 07/28/16 Pct Recovery = 75% Analysis Date = 07/23/16 Pct Recovery = 75% Analysis Date = 07/23/16 Pct Recovery = 75% Analysis Date = 07/18/16 Pct Recovery = 76% Analysis Date = 07/18/16 Pct Recovery = 76% Analysis Date = 07/14/16 Pct Recovery = 76% Analysis Date = 07/14/16 Pct Recovery = 76% Analysis Date = 07/09/16 Pct Recovery = 76% Analysis Date = 07/09/16 Pct Recovery = 76% Analysis Date = 07/04/16 Pct Recovery = 76% Analysis Date = 07/04/16 Pct Recovery = 76% Analysis Date = 06/29/16 Pct Recovery = 77% Analysis Date = 06/29/16 Pct Recovery = 77% Analysis Date = 06/24/16 Pct Recovery = 77% Analysis Date = 06/24/16 Pct Recovery = 77% Analysis Date = 06/19/16 Pct Recovery = 77% Analysis Date = 06/19/16 Pct Recovery = 77% Analysis Date = 06/15/16 Pct Recovery = 78% Analysis Date = 06/15/16 Pct Recovery = 78% Analysis Date = 06/10/16 Pct Recovery = 78% Analysis Date = 06/10/16 Pct Recovery = 78% Analysis Date = 06/05/16 Pct Recovery = 78% Analysis Date = 06/05/16 Pct Recovery = 78% Analysis Date = 05/31/16 Pct Recovery = 79% Analysis Date = 05/31/16 Pct Recovery = 79% Analysis Date = 05/26/16 Pct Recovery = 79% Analysis Date = 05/26/16 Pct Recovery = 79% Analysis Date = 05/21/16 Pct Recovery = 79% Analysis Date = 05/21/16 Pct Recovery = 79% Analysis Date = 05/17/16 Pct Recovery = 80% Analysis Date = 05/17/16 Pct Recovery = 80% Analysis Date = 05/12/16 Pct Recovery = 80% Analysis Date = 05/12/16 Pct Recovery = 80% Analysis Date = 05/07/16 Pct Recovery = 80% Analysis Date = 05/07/16 Pct Recovery = 80% Analysis Date = 05/02/16 Pct Recovery = 81% Analysis Date = 05/02/16 Pct Recovery = 81% Analysis Date = 04/27/16 Pct Recovery = 81% Analysis Date = 04/27/16 Pct Recovery = 81% Analysis Date = 04/22/16 Pct Recovery = 81% Analysis Date = 04/22/16 Pct Recovery = 81% Analysis Date = 04/18/16 Pct Recovery = 82% Analysis Date = 04/18/16 Pct Recovery = 82% Analysis Date = 04/13/16 Pct Recovery = 82% Analysis Date = 04/13/16 Pct Recovery = 82% Analysis Date = 04/08/16 Pct Recovery = 82% Analysis Date = 04/08/16 Pct Recovery = 82% Analysis Date = 04/03/16 Pct Recovery = 83% Analysis Date = 04/03/16 Pct Recovery = 83% Analysis Date = 03/29/16 Pct Recovery = 83% Analysis Date = 03/29/16 Pct Recovery = 83% Analysis Date = 03/24/16 Pct Recovery = 83% Analysis Date = 03/24/16 Pct Recovery = 83% Analysis Date = 03/19/16 Pct Recovery = 83% Analysis Date = 03/19/16 Pct Recovery = 83% Analysis Date = 03/15/16 Pct Recovery = 84% Analysis Date = 03/15/16 Pct Recovery = 84% Analysis Date = 03/10/16 Pct Recovery = 84% Analysis Date = 03/10/16 Pct Recovery = 84% Analysis Date = 03/05/16 Pct Recovery = 84% Analysis Date = 03/05/16 Pct Recovery = 84% Analysis Date = 02/29/16 Pct Recovery = 85% Analysis Date = 02/29/16 Pct Recovery = 85% Analysis Date = 02/24/16 Pct Recovery = 85% Analysis Date = 02/24/16 Pct Recovery = 85% Analysis Date = 02/19/16 Pct Recovery = 85% Analysis Date = 02/19/16 Pct Recovery = 85% Analysis Date = 02/15/16 Pct Recovery = 86% Analysis Date = 02/15/16 Pct Recovery = 86% Analysis Date = 02/10/16 Pct Recovery = 86% Analysis Date = 02/10/16 Pct Recovery = 86% Analysis Date = 02/05/16 Pct Recovery = 86% Analysis Date = 02/05/16 Pct Recovery = 86% Analysis Date = 01/31/16 Pct Recovery = 86% Analysis Date = 01/31/16 Pct Recovery = 86% Analysis Date = 01/26/16 Pct Recovery = 87% Analysis Date = 01/26/16 Pct Recovery = 87% Analysis Date = 01/21/16 Pct Recovery = 87% Analysis Date = 01/21/16 Pct Recovery = 87% Analysis Date = 01/17/16 Pct Recovery = 87% Analysis Date = 01/17/16 Pct Recovery = 87% Analysis Date = 01/12/16 Pct Recovery = 87% Analysis Date = 01/12/16 Pct Recovery = 87% Analysis Date = 01/07/16 Pct Recovery = 88% Analysis Date = 01/07/16 Pct Recovery = 88% Analysis Date = 01/02/16 Pct Recovery = 88% Analysis Date = 01/02/16 Pct Recovery = 88% Analysis Date = 12/28/15 Pct Recovery = 88% Analysis Date = 12/28/15 Pct Recovery = 88% Analysis Date = 12/23/15 Pct Recovery = 88% Analysis Date = 12/23/15 Pct Recovery = 88% Analysis Date = 12/19/15 Pct Recovery = 89% Analysis Date = 12/19/15 Pct Recovery = 89% Analysis Date = 12/14/15 Pct Recovery = 89% Analysis Date = 12/14/15 Pct Recovery = 89% Analysis Date = 12/09/15 Pct Recovery = 89% Analysis Date = 12/09/15 Pct Recovery = 89% Analysis Date = 12/04/15 Pct Recovery = 89% Analysis Date = 12/04/15 Pct Recovery = 89% Analysis Date = 11/29/15 Pct Recovery = 90% Analysis Date = 11/29/15 Pct Recovery = 90% Analysis Date = 11/24/15 Pct Recovery = 90% Analysis Date = 11/24/15 Pct Recovery = 90% Analysis Date = 11/19/15 Pct Recovery = 90% Analysis Date = 11/19/15 Pct Recovery = 90% Analysis Date = 11/15/15 Pct Recovery = 90% Analysis Date = 11/15/15 Pct Recovery = 90% Analysis Date = 11/10/15 Pct Recovery = 90% Analysis Date = 11/10/15 Pct Recovery = 90% Analysis Date = 11/05/15 Pct Recovery = 90% Analysis Date = 11/05/15 Pct Recovery = 90% Analysis Date = 10/31/15 Pct Recovery = 90% Analysis Date = 10/31/15 Pct Recovery = 90% Analysis Date = 10/26/15 Pct Recovery = 90% Analysis Date = 10/26/15 Pct Recovery = 90% Analysis Date = 10/21/15 Pct Recovery = 90% Analysis Date = 10/21/15 Pct Recovery = 90% Analysis Date = 10/17/15 Pct Recovery = 90% Analysis Date = 10/17/15 Pct Recovery = 90% Analysis Date = 10/12/15 Pct Recovery = 91% Analysis Date = 10/12/15 Pct Recovery = 91% Analysis Date = 10/07/15 Pct Recovery = 91% Analysis Date = 10/07/15 Pct Recovery = 91% Analysis Date = 10/02/15 Pct Recovery = 91% Analysis Date = 10/02/15 Pct Recovery = 91% Analysis Date = 09/27/15 Pct Recovery = 91% Analysis Date = 09/27/15 Pct Recovery = 91% Analysis Date = 09/22/15 Pct Recovery = 91% Analysis Date = 09/22/15 Pct Recovery = 91% Analysis Date = 09/18/15 Pct Recovery = 91% Analysis Date = 09/18/15 Pct Recovery = 91% Analysis Date = 09/13/15 Pct Recovery = 91% Analysis Date = 09/13/15 Pct Recovery = 91% Analysis Date = 09/08/15 Pct Recovery = 91% Analysis Date = 09/08/15 Pct Recovery = 91% Analysis Date = 09/03/15 Pct Recovery = 91% Analysis Date = 09/03/15 Pct Recovery = 91% Analysis Date = 08/29/15 Pct Recovery = 91% Analysis Date = 08/29/15 Pct Recovery = 91% Analysis Date = 08/24/15 Pct Recovery = 91% Analysis Date = 08/24/15 Pct Recovery = 91% Analysis Date = 08/20/15 Pct Recovery = 92% Analysis Date = 08/20/15 Pct Recovery = 92% Analysis Date = 08/15/15 Pct Recovery = 92% Analysis Date = 08/15/15 Pct Recovery = 92% Analysis Date = 08/10/15 Pct Recovery = 92% Analysis Date = 08/10/15 Pct Recovery = 92% Analysis Date = 08/05/15 Pct Recovery = 92% Analysis Date = 08/05/15 Pct Recovery = 92% Analysis Date = 07/31/15 Pct Recovery = 92% Analysis Date = 07/31/15 Pct Recovery = 92% Analysis Date = 07/26/15 Pct Recovery = 92% Analysis Date = 07/26/15 Pct Recovery = 92% Analysis Date = 07/21/15 Pct Recovery = 92% Analysis Date = 07/21/15 Pct Recovery = 92% Analysis Date = 07/17/15 Pct Recovery = 92% Analysis Date = 07/17/15 Pct Recovery = 92% Analysis Date = 07/12/15 Pct Recovery = 92% Analysis Date = 07/12/15 Pct Recovery = 92% Analysis Date = 07/07/15 Pct Recovery = 92% Analysis Date = 07/07/15 Pct Recovery = 92% Analysis Date = 07/02/15 Pct Recovery = 93% Analysis Date = 07/02/15 Pct Recovery = 93% Analysis Date = 06/27/15 Pct Recovery = 93% Analysis Date = 06/27/15 Pct Recovery = 93% Analysis Date = 06/22/15 Pct Recovery = 93% Analysis Date = 06/22/15 Pct Recovery = 93% Analysis Date = 06/18/15 Pct Recovery = 93% Analysis Date = 06/18/15 Pct Recovery = 93% Analysis Date = 06/13/15 Pct Recovery = 93% Analysis Date = 06/13/15 Pct Recovery = 93% Analysis Date = 06/08/15 Pct Recovery = 94% Analysis Date = 06/08/15 Pct Recovery = 94% Analysis Date = 06/03/15 Pct Recovery = 94% Analysis Date = 06/03/15 Pct Recovery = 94% Analysis Date = 05/29/15 Pct Recovery = 94% Analysis Date = 05/29/15 Pct Recovery = 94% Analysis Date = 05/24/15 Pct Recovery = 94% Analysis Date = 05/24/15 Pct Recovery = 94% Analysis Date = 05/20/15 Pct Recovery = 95% Analysis Date = 05/20/15 Pct Recovery = 95% Analysis Date = 05/15/15 Pct Recovery = 95% Analysis Date = 05/15/15 Pct Recovery = 95% Analysis Date = 05/10/15 Pct Recovery = 95% Analysis Date = 05/10/15 Pct Recovery = 95% Analysis Date = 05/05/15 Pct Recovery = 95% Analysis Date = 05/05/15 Pct Recovery = 95% Analysis Date = 04/30/15 Pct Recovery = 95% Analysis Date = 04/30/15 Pct Recovery = 95% Analysis Date = 04/25/15 Pct Recovery = 96% Analysis Date = 04/25/15 Pct Recovery = 96% Analysis Date = 04/21/15 Pct Recovery = 96% Analysis Date = 04/21/15 Pct Recovery = 96% Analysis Date = 04/16/15 Pct Recovery = 96% Analysis Date = 04/16/15 Pct Recovery = 96% Analysis Date = 04/11/15 Pct Recovery = 96% Analysis Date = 04/11/15 Pct Recovery = 96% Analysis Date = 04/06/15 Pct Recovery = 97% Analysis Date = 04/06/15 Pct Recovery = 97% Analysis Date = 04/01/15 Pct Recovery = 97% Analysis Date = 04/01/15 Pct Recovery = 97% Analysis Date = 03/27/15 Pct Recovery = 97% Analysis Date = 03/27/15 Pct Recovery = 97% Analysis Date = 03/22/15 Pct Recovery = 97% Analysis Date = 03/22/15 Pct Recovery = 97% Analysis Date = 03/18/15 Pct Recovery = 98% Analysis Date = 03/18/15 Pct Recovery = 98% Analysis Date = 03/13/15 Pct Recovery = 98% Analysis Date = 03/13/15 Pct Recovery = 98% Analysis Date = 03/08/15 Pct Recovery = 98% Analysis Date = 03/08/15 Pct Recovery = 98% Analysis Date = 03/03/15 Pct Recovery = 98% Analysis Date = 03/03/15 Pct Recovery = 98% Analysis Date = 02/26/15 Pct Recovery = 98% Analysis Date = 02/26/15 Pct Recovery = 98% Analysis Date = 02/21/15 Pct Recovery = 98% Analysis Date = 02/21/15 Pct Recovery = 98% Analysis Date = 02/17/15 Pct Recovery = 98% Analysis Date = 02/17/15 Pct Recovery = 98% Analysis Date = 02/12/15 Pct Recovery = 98% Analysis Date = 02/12/15 Pct Recovery = 98% Analysis Date = 02/07/15 Pct Recovery = 97% Analysis Date = 02/07/15 Pct Recovery = 97% Analysis Date = 02/02/15 Pct Recovery = 97% Analysis Date = 02/02/15 Pct Recovery = 97% Analysis Date = 01/28/15 Pct Recovery = 97% Analysis Date = 01/28/15 Pct Recovery = 97% Analysis Date = 01/23/15 Pct Recovery = 97% Analysis Date = 01/23/15 Pct Recovery = 97% Analysis Date = 01/19/15 Pct Recovery = 97% Analysis Date = 01/19/15 Pct Recovery = 97% Analysis Date = 01/14/15 Pct Recovery = 97% Analysis Date = 01/14/15 Pct Recovery = 97% Analysis Date = 01/09/15 Pct Recovery = 97% Analysis Date = 01/09/15 Pct Recovery = 97% Analysis Date = 01/04/15 Pct Recovery = 97% Analysis Date = 01/04/15 Pct Recovery = 97% Analysis Date = 12/30/14 Pct Recovery = 97% Analysis Date = 12/30/14 Pct Recovery = 97% Analysis Date = 12/25/14 Pct Recovery = 97% Analysis Date = 12/25/14 Pct Recovery = 97% Analysis Date = 12/21/14 Pct Recovery = 97% Analysis Date = 12/21/14 Pct Recovery = 97% Analysis Date = 12/16/14 Pct Recovery = 97% Analysis Date = 12/16/14 Pct Recovery = 97% Analysis Date = 12/11/14 Pct Recovery = 97% Analysis Date = 12/11/14 Pct Recovery = 97% Analysis Date = 12/06/14 Pct Recovery = 97% Analysis Date = 12/06/14 Pct Recovery = 97% Analysis Date = 12/01/14 Pct Recovery = 97% Analysis Date = 12/01/14 Pct Recovery = 97% Analysis Date = 11/26/14 Pct Recovery = 97% Analysis Date = 11/26/14 Pct Recovery = 97% Analysis Date = 11/21/14 Pct Recovery = 96% Analysis Date = 11/21/14 Pct Recovery = 96% Analysis Date = 11/17/14 Pct Recovery = 96% Analysis Date = 11/17/14 Pct Recovery = 96% Analysis Date = 11/12/14 Pct Recovery = 96% Analysis Date = 11/12/14 Pct Recovery = 96% Analysis Date = 11/07/14 Pct Recovery = 96% Analysis Date = 11/07/14 Pct Recovery = 96% Analysis Date = 11/02/14 Pct Recovery = 96% Analysis Date = 11/02/14 Pct Recovery = 96% Analysis Date = 10/28/14 Pct Recovery = 96% Analysis Date = 10/28/14 Pct Recovery = 96% Analysis Date = 10/23/14 Pct Recovery = 96% Analysis Date = 10/23/14 Pct Recovery = 96% Analysis Date = 10/19/14 Pct Recovery = 96% Analysis Date = 10/19/14 Pct Recovery = 96% Analysis Date = 10/14/14 Pct Recovery = 96% Analysis Date = 10/14/14 Pct Recovery = 96% Analysis Date = 10/09/14 Pct Recovery = 96% Analysis Date = 10/09/14 Pct Recovery = 96% Analysis Date = 10/04/14 Pct Recovery = 96% Analysis Date = 10/04/14 Pct Recovery = 96% Analysis Date = 09/29/14 Pct Recovery = 96% Analysis Date = 09/29/14 Pct Recovery = 96% Analysis Date = 09/24/14 Pct Recovery = 96% Analysis Date = 09/24/14 Pct Recovery = 96% Analysis Date = 09/20/14 Pct Recovery = 96% Analysis Date = 09/20/14 Pct Recovery = 96% Analysis Date = 09/15/14 Pct Recovery = 96% Analysis Date = 09/15/14 Pct Recovery = 96% Analysis Date = 09/10/14 Pct Recovery = 96% Analysis Date = 09/10/14 Pct Recovery = 96% Analysis Date = 09/05/14 Pct Recovery = 96% Analysis Date = 09/05/14 Pct Recovery = 96% Analysis Date = 08/31/14 Pct Recovery = 95% Analysis Date = 08/31/14 Pct Recovery = 95% Analysis Date = 08/26/14 Pct Recovery = 95% Analysis Date = 08/26/14 Pct Recovery = 95% Analysis Date = 08/22/14 Pct Recovery = 95% Analysis Date = 08/22/14 Pct Recovery = 95% Analysis Date = 08/17/14 Pct Recovery = 95% Analysis Date = 08/17/14 Pct Recovery = 95% Analysis Date = 08/12/14 Pct Recovery = 95% Analysis Date = 08/12/14 Pct Recovery = 95% Analysis Date = 08/07/14 Pct Recovery = 95% Analysis Date = 08/07/14 Pct Recovery = 95% Analysis Date = 08/02/14 Pct Recovery = 95% Analysis Date = 08/02/14 Pct Recovery = 95% Analysis Date = 07/28/14 Pct Recovery = 95% Analysis Date = 07/28/14 Pct Recovery = 95% Analysis Date = 07/23/14 Pct Recovery = 95% Analysis Date = 07/23/14 Pct Recovery = 95% Analysis Date = 07/19/14 Pct Recovery = 95% Analysis Date = 07/19/14 Pct Recovery = 95% Analysis Date = 07/14/14 Pct Recovery = 95% Analysis Date = 07/14/14 Pct Recovery = 95% Analysis Date = 07/09/14 Pct Recovery = 95% Analysis Date = 07/09/14 Pct Recovery = 95% Analysis Date = 07/04/14 Pct Recovery = 95% Analysis Date = 07/04/14 Pct Recovery = 95% Analysis Date = 06/29/14 Pct Recovery = 95% Analysis Date = 06/29/14 Pct Recovery = 95% Analysis Date = 06/24/14 Pct Recovery = 95% Analysis Date = 06/24/14 Pct Recovery = 95% Analysis Date = 06/20/14 Pct Recovery = 95% Analysis Date = 06/20/14 Pct Recovery = 95% Analysis Date = 06/15/14 Pct Recovery = 95% Analysis Date = 06/15/14 Pct Recovery = 95% Analysis Date = 06/10/14 Pct Recovery = 95% Analysis Date = 06/10/14 Pct Recovery = 95% Analysis Date = 06/05/14 Pct Recovery = 95% Analysis Date = 06/05/14 Pct Recovery = 95% Analysis Date = 05/31/14 Pct Recovery = 95% Analysis Date = 05/31/14 Pct Recovery = 95% Analysis Date = 05/26/14 Pct Recovery = 95% Analysis Date = 05/26/14 Pct Recovery = 95% Analysis Date = 05/22/14 Pct Recovery = 95% Analysis Date = 05/22/14 Pct Recovery = 95% Analysis Date = 05/17/14 Pct Recovery = 95% Analysis Date = 05/17/14 Pct Recovery = 95% Analysis Date = 05/12/14 Pct Recovery = 95% Analysis Date = 05/12/14 Pct Recovery = 95% Analysis Date = 05/07/14 Pct Recovery = 95% Analysis Date = 05/07/14 Pct Recovery = 95% Analysis Date = 05/02/14 Pct Recovery = 95% Analysis Date = 05/02/14 Pct Recovery = 95% Analysis Date = 04/27/14 Pct Recovery = 95% Analysis Date = 04/27/14 Pct Recovery = 95% Analysis Date = 04/23/14 Pct Recovery = 95% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
PENCICLOVIR

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 1 142% . 142% 0%
>= Reporting Level 63 85% 30% 76% 35%
Total 64 86% 31% 76% 35%

Sample Statistics
PENCICLOVIR

Characteristic N % % Basis
Plotted 64 84% Spiked
Estimated Values 24 32% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 8 11% Spiked
Spiked 76 .  
False Negatives 4 5% 4 out of 76
Not Spiked 39 .  
False Positives 0 0% 0 out of 39

BQS OBSP Determination:
PENTOXIFYLLINE
METHOD: 2440 , TESTIDCODE: 67480LCM56
Open Data Set

Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 78% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 77% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 73% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 76% Analysis Date = 01/17/16 SpikeMix = ERA 0406-15-09: 80 µl & ERA 0406-15-07A: 80 µl Pct Recovery = 76% Analysis Date = 11/24/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 76% Analysis Date = 10/01/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 82% Analysis Date = 11/05/15 SpikeMix = ERA 0406-15-08: 80 µl & Abs 052215: 80 µl Pct Recovery = 80% Analysis Date = 11/04/15 SpikeMix = Abs 052215: 80 µl & Abs 050115: 80 µl Pct Recovery = 81% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 69% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 71% Analysis Date = 09/24/16 SpikeMix = Crescent EN160610015: 80 µl & Abs 061416: 80 µl Pct Recovery = 71% Analysis Date = 09/24/16 SpikeMix = Abs 061416: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 76% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 71% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 72% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 87% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 87% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-04: 15 µl & Abs 041814: 15 µl Pct Recovery = 78% Analysis Date = 12/06/14 SpikeMix = ERA 0318-14-02: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 74% Analysis Date = 10/25/14 SpikeMix = Abs 041614: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 72% Analysis Date = 10/11/14 SpikeMix = ERA 0318-14-02: 60 µl & ERA 0319-14-04: 60 µl Pct Recovery = 61% Analysis Date = 08/28/14 SpikeMix = ERA 0319-14-04: 60 µl & ERA 0319-14-05: 60 µl Pct Recovery = 63% Analysis Date = 05/07/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 99% Analysis Date = 03/11/15 SpikeMix = ERA 0318-14-02: 15 µl & Abs 041714: 15 µl Pct Recovery = 87% Analysis Date = 01/16/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 86% Analysis Date = 12/06/14 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 64% Analysis Date = 08/21/14 SpikeMix = ERA 0318-14-02: 60 µl & Abs 041714: 60 µl Pct Recovery = 42% Analysis Date = 07/12/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 45% Analysis Date = 06/11/14 SpikeMix = Abs 041614: 60 µl & Abs 041714: 60 µl Pct Recovery = 52% Analysis Date = 05/21/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 51% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-08: 40 µl & ERA 0406-15-09: 40 µl Pct Recovery = 87% Analysis Date = 07/31/15 SpikeMix = ERA 0406-15-09: 40 µl & Abs 050115: 40 µl Pct Recovery = 93% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-08: 40 µl & Abs 052215: 40 µl Pct Recovery = 82% Analysis Date = 02/23/16 SpikeMix = Abs 052215: 40 µl & Abs 050115: 40 µl Pct Recovery = 80% Analysis Date = 09/10/15 SpikeMix = Abs 052215: 40 µl & ERA 0406-15-07A: 40 µl Pct Recovery = 84% Analysis Date = 07/31/15 SpikeMix = Abs 051315: 40 µl & Abs 052215: 40 µl Pct Recovery = 61% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 74% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 73% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 81% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 85% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 69% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 71% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 76% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 71% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 64% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 64% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 68% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 53% Analysis Date = 04/30/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 79% Analysis Date = 04/10/15 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 74% Analysis Date = 02/10/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 84% Analysis Date = 12/07/14 SpikeMix = ERA 0318-14-02: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 68% Analysis Date = 10/11/14 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 41% Analysis Date = 11/04/14 SpikeMix = Abs 041714: 8 µl & ERA 0319-14-05: 8 µl Pct Recovery = 57% Analysis Date = 04/23/14 SpikeMix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.2: 20 µl Pct Recovery = 55% Analysis Date = 09/12/14 SpikeMix = Abs 041614: 30 µl & ERA 0319-14-04: 30 µl Pct Recovery = 44% Analysis Date = 10/10/14 SpikeMix = Abs 041714: 30 µl & Abs 041814: 30 µl Pct Recovery = 50% Analysis Date = 07/20/14 SpikeMix = ERA 0318-14-02: 30 µl & Abs 041714: 30 µl Pct Recovery = 52% Analysis Date = 05/17/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 51% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 83% Analysis Date = 11/24/15 SpikeMix = ERA 0406-15-09: 20 µl & Abs 050115: 20 µl Pct Recovery = 95% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 81% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 78% Analysis Date = 02/23/16 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 79% Analysis Date = 07/09/15 SpikeMix = Abs 050115: 20 µl & Abs 052215: 20 µl Pct Recovery = 75% Analysis Date = 06/26/15 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 93% Analysis Date = 04/09/16 SpikeMix = Abs 051315: 10 µl & ERA 0406-15-09: 10 µl Pct Recovery = 48% Analysis Date = 04/09/16 SpikeMix = Abs 051315: 10 µl & ERA 0406-15-09: 10 µl Pct Recovery = 52% Analysis Date = 01/18/17 Pct Recovery = 73% Analysis Date = 01/13/17 Pct Recovery = 73% Analysis Date = 01/13/17 Pct Recovery = 73% Analysis Date = 01/08/17 Pct Recovery = 73% Analysis Date = 01/08/17 Pct Recovery = 73% Analysis Date = 01/03/17 Pct Recovery = 73% Analysis Date = 01/03/17 Pct Recovery = 73% Analysis Date = 12/29/16 Pct Recovery = 73% Analysis Date = 12/29/16 Pct Recovery = 73% Analysis Date = 12/24/16 Pct Recovery = 73% Analysis Date = 12/24/16 Pct Recovery = 73% Analysis Date = 12/19/16 Pct Recovery = 73% Analysis Date = 12/19/16 Pct Recovery = 73% Analysis Date = 12/14/16 Pct Recovery = 73% Analysis Date = 12/14/16 Pct Recovery = 73% Analysis Date = 12/09/16 Pct Recovery = 73% Analysis Date = 12/09/16 Pct Recovery = 73% Analysis Date = 12/04/16 Pct Recovery = 73% Analysis Date = 12/04/16 Pct Recovery = 73% Analysis Date = 11/29/16 Pct Recovery = 73% Analysis Date = 11/29/16 Pct Recovery = 73% Analysis Date = 11/24/16 Pct Recovery = 73% Analysis Date = 11/24/16 Pct Recovery = 73% Analysis Date = 11/19/16 Pct Recovery = 73% Analysis Date = 11/19/16 Pct Recovery = 73% Analysis Date = 11/14/16 Pct Recovery = 73% Analysis Date = 11/14/16 Pct Recovery = 73% Analysis Date = 11/09/16 Pct Recovery = 73% Analysis Date = 11/09/16 Pct Recovery = 73% Analysis Date = 11/04/16 Pct Recovery = 73% Analysis Date = 11/04/16 Pct Recovery = 73% Analysis Date = 10/30/16 Pct Recovery = 73% Analysis Date = 10/30/16 Pct Recovery = 73% Analysis Date = 10/25/16 Pct Recovery = 73% Analysis Date = 10/25/16 Pct Recovery = 73% Analysis Date = 10/20/16 Pct Recovery = 73% Analysis Date = 10/20/16 Pct Recovery = 73% Analysis Date = 10/15/16 Pct Recovery = 73% Analysis Date = 10/15/16 Pct Recovery = 73% Analysis Date = 10/10/16 Pct Recovery = 73% Analysis Date = 10/10/16 Pct Recovery = 73% Analysis Date = 10/05/16 Pct Recovery = 73% Analysis Date = 10/05/16 Pct Recovery = 73% Analysis Date = 09/30/16 Pct Recovery = 73% Analysis Date = 09/30/16 Pct Recovery = 73% Analysis Date = 09/25/16 Pct Recovery = 73% Analysis Date = 09/25/16 Pct Recovery = 73% Analysis Date = 09/20/16 Pct Recovery = 73% Analysis Date = 09/20/16 Pct Recovery = 73% Analysis Date = 09/15/16 Pct Recovery = 73% Analysis Date = 09/15/16 Pct Recovery = 73% Analysis Date = 09/10/16 Pct Recovery = 73% Analysis Date = 09/10/16 Pct Recovery = 73% Analysis Date = 09/05/16 Pct Recovery = 73% Analysis Date = 09/05/16 Pct Recovery = 73% Analysis Date = 08/31/16 Pct Recovery = 73% Analysis Date = 08/31/16 Pct Recovery = 73% Analysis Date = 08/26/16 Pct Recovery = 73% Analysis Date = 08/26/16 Pct Recovery = 73% Analysis Date = 08/21/16 Pct Recovery = 73% Analysis Date = 08/21/16 Pct Recovery = 73% Analysis Date = 08/16/16 Pct Recovery = 73% Analysis Date = 08/16/16 Pct Recovery = 73% Analysis Date = 08/11/16 Pct Recovery = 73% Analysis Date = 08/11/16 Pct Recovery = 73% Analysis Date = 08/06/16 Pct Recovery = 73% Analysis Date = 08/06/16 Pct Recovery = 73% Analysis Date = 08/01/16 Pct Recovery = 73% Analysis Date = 08/01/16 Pct Recovery = 73% Analysis Date = 07/27/16 Pct Recovery = 74% Analysis Date = 07/27/16 Pct Recovery = 74% Analysis Date = 07/22/16 Pct Recovery = 74% Analysis Date = 07/22/16 Pct Recovery = 74% Analysis Date = 07/17/16 Pct Recovery = 74% Analysis Date = 07/17/16 Pct Recovery = 74% Analysis Date = 07/12/16 Pct Recovery = 74% Analysis Date = 07/12/16 Pct Recovery = 74% Analysis Date = 07/07/16 Pct Recovery = 74% Analysis Date = 07/07/16 Pct Recovery = 74% Analysis Date = 07/02/16 Pct Recovery = 74% Analysis Date = 07/02/16 Pct Recovery = 74% Analysis Date = 06/27/16 Pct Recovery = 74% Analysis Date = 06/27/16 Pct Recovery = 74% Analysis Date = 06/22/16 Pct Recovery = 74% Analysis Date = 06/22/16 Pct Recovery = 74% Analysis Date = 06/17/16 Pct Recovery = 74% Analysis Date = 06/17/16 Pct Recovery = 74% Analysis Date = 06/12/16 Pct Recovery = 74% Analysis Date = 06/12/16 Pct Recovery = 74% Analysis Date = 06/07/16 Pct Recovery = 74% Analysis Date = 06/07/16 Pct Recovery = 74% Analysis Date = 06/02/16 Pct Recovery = 74% Analysis Date = 06/02/16 Pct Recovery = 74% Analysis Date = 05/28/16 Pct Recovery = 74% Analysis Date = 05/28/16 Pct Recovery = 74% Analysis Date = 05/23/16 Pct Recovery = 74% Analysis Date = 05/23/16 Pct Recovery = 74% Analysis Date = 05/18/16 Pct Recovery = 74% Analysis Date = 05/18/16 Pct Recovery = 74% Analysis Date = 05/13/16 Pct Recovery = 74% Analysis Date = 05/13/16 Pct Recovery = 74% Analysis Date = 05/08/16 Pct Recovery = 74% Analysis Date = 05/08/16 Pct Recovery = 74% Analysis Date = 05/03/16 Pct Recovery = 74% Analysis Date = 05/03/16 Pct Recovery = 74% Analysis Date = 04/28/16 Pct Recovery = 75% Analysis Date = 04/28/16 Pct Recovery = 75% Analysis Date = 04/23/16 Pct Recovery = 75% Analysis Date = 04/23/16 Pct Recovery = 75% Analysis Date = 04/18/16 Pct Recovery = 75% Analysis Date = 04/18/16 Pct Recovery = 75% Analysis Date = 04/13/16 Pct Recovery = 75% Analysis Date = 04/13/16 Pct Recovery = 75% Analysis Date = 04/08/16 Pct Recovery = 75% Analysis Date = 04/08/16 Pct Recovery = 75% Analysis Date = 04/03/16 Pct Recovery = 75% Analysis Date = 04/03/16 Pct Recovery = 75% Analysis Date = 03/29/16 Pct Recovery = 76% Analysis Date = 03/29/16 Pct Recovery = 76% Analysis Date = 03/24/16 Pct Recovery = 76% Analysis Date = 03/24/16 Pct Recovery = 76% Analysis Date = 03/19/16 Pct Recovery = 76% Analysis Date = 03/19/16 Pct Recovery = 76% Analysis Date = 03/14/16 Pct Recovery = 76% Analysis Date = 03/14/16 Pct Recovery = 76% Analysis Date = 03/09/16 Pct Recovery = 76% Analysis Date = 03/09/16 Pct Recovery = 76% Analysis Date = 03/04/16 Pct Recovery = 76% Analysis Date = 03/04/16 Pct Recovery = 76% Analysis Date = 02/28/16 Pct Recovery = 76% Analysis Date = 02/28/16 Pct Recovery = 76% Analysis Date = 02/23/16 Pct Recovery = 77% Analysis Date = 02/23/16 Pct Recovery = 77% Analysis Date = 02/18/16 Pct Recovery = 77% Analysis Date = 02/18/16 Pct Recovery = 77% Analysis Date = 02/13/16 Pct Recovery = 77% Analysis Date = 02/13/16 Pct Recovery = 77% Analysis Date = 02/08/16 Pct Recovery = 77% Analysis Date = 02/08/16 Pct Recovery = 77% Analysis Date = 02/03/16 Pct Recovery = 77% Analysis Date = 02/03/16 Pct Recovery = 77% Analysis Date = 01/29/16 Pct Recovery = 77% Analysis Date = 01/29/16 Pct Recovery = 77% Analysis Date = 01/24/16 Pct Recovery = 77% Analysis Date = 01/24/16 Pct Recovery = 77% Analysis Date = 01/19/16 Pct Recovery = 78% Analysis Date = 01/19/16 Pct Recovery = 78% Analysis Date = 01/14/16 Pct Recovery = 78% Analysis Date = 01/14/16 Pct Recovery = 78% Analysis Date = 01/09/16 Pct Recovery = 78% Analysis Date = 01/09/16 Pct Recovery = 78% Analysis Date = 01/04/16 Pct Recovery = 78% Analysis Date = 01/04/16 Pct Recovery = 78% Analysis Date = 12/30/15 Pct Recovery = 78% Analysis Date = 12/30/15 Pct Recovery = 78% Analysis Date = 12/25/15 Pct Recovery = 78% Analysis Date = 12/25/15 Pct Recovery = 78% Analysis Date = 12/20/15 Pct Recovery = 78% Analysis Date = 12/20/15 Pct Recovery = 78% Analysis Date = 12/15/15 Pct Recovery = 79% Analysis Date = 12/15/15 Pct Recovery = 79% Analysis Date = 12/10/15 Pct Recovery = 79% Analysis Date = 12/10/15 Pct Recovery = 79% Analysis Date = 12/05/15 Pct Recovery = 79% Analysis Date = 12/05/15 Pct Recovery = 79% Analysis Date = 11/30/15 Pct Recovery = 79% Analysis Date = 11/30/15 Pct Recovery = 79% Analysis Date = 11/25/15 Pct Recovery = 79% Analysis Date = 11/25/15 Pct Recovery = 79% Analysis Date = 11/20/15 Pct Recovery = 79% Analysis Date = 11/20/15 Pct Recovery = 79% Analysis Date = 11/15/15 Pct Recovery = 79% Analysis Date = 11/15/15 Pct Recovery = 79% Analysis Date = 11/10/15 Pct Recovery = 79% Analysis Date = 11/10/15 Pct Recovery = 79% Analysis Date = 11/05/15 Pct Recovery = 79% Analysis Date = 11/05/15 Pct Recovery = 79% Analysis Date = 10/31/15 Pct Recovery = 79% Analysis Date = 10/31/15 Pct Recovery = 79% Analysis Date = 10/26/15 Pct Recovery = 79% Analysis Date = 10/26/15 Pct Recovery = 79% Analysis Date = 10/21/15 Pct Recovery = 79% Analysis Date = 10/21/15 Pct Recovery = 79% Analysis Date = 10/16/15 Pct Recovery = 79% Analysis Date = 10/16/15 Pct Recovery = 79% Analysis Date = 10/11/15 Pct Recovery = 79% Analysis Date = 10/11/15 Pct Recovery = 79% Analysis Date = 10/06/15 Pct Recovery = 79% Analysis Date = 10/06/15 Pct Recovery = 79% Analysis Date = 10/01/15 Pct Recovery = 79% Analysis Date = 10/01/15 Pct Recovery = 79% Analysis Date = 09/26/15 Pct Recovery = 79% Analysis Date = 09/26/15 Pct Recovery = 79% Analysis Date = 09/21/15 Pct Recovery = 79% Analysis Date = 09/21/15 Pct Recovery = 79% Analysis Date = 09/16/15 Pct Recovery = 79% Analysis Date = 09/16/15 Pct Recovery = 79% Analysis Date = 09/11/15 Pct Recovery = 79% Analysis Date = 09/11/15 Pct Recovery = 79% Analysis Date = 09/05/15 Pct Recovery = 79% Analysis Date = 09/05/15 Pct Recovery = 79% Analysis Date = 08/31/15 Pct Recovery = 79% Analysis Date = 08/31/15 Pct Recovery = 79% Analysis Date = 08/26/15 Pct Recovery = 79% Analysis Date = 08/26/15 Pct Recovery = 79% Analysis Date = 08/21/15 Pct Recovery = 79% Analysis Date = 08/21/15 Pct Recovery = 79% Analysis Date = 08/16/15 Pct Recovery = 79% Analysis Date = 08/16/15 Pct Recovery = 79% Analysis Date = 08/11/15 Pct Recovery = 79% Analysis Date = 08/11/15 Pct Recovery = 79% Analysis Date = 08/06/15 Pct Recovery = 79% Analysis Date = 08/06/15 Pct Recovery = 79% Analysis Date = 08/01/15 Pct Recovery = 79% Analysis Date = 08/01/15 Pct Recovery = 79% Analysis Date = 07/27/15 Pct Recovery = 79% Analysis Date = 07/27/15 Pct Recovery = 79% Analysis Date = 07/22/15 Pct Recovery = 79% Analysis Date = 07/22/15 Pct Recovery = 79% Analysis Date = 07/17/15 Pct Recovery = 79% Analysis Date = 07/17/15 Pct Recovery = 79% Analysis Date = 07/12/15 Pct Recovery = 79% Analysis Date = 07/12/15 Pct Recovery = 79% Analysis Date = 07/07/15 Pct Recovery = 79% Analysis Date = 07/07/15 Pct Recovery = 79% Analysis Date = 07/02/15 Pct Recovery = 79% Analysis Date = 07/02/15 Pct Recovery = 79% Analysis Date = 06/27/15 Pct Recovery = 79% Analysis Date = 06/27/15 Pct Recovery = 79% Analysis Date = 06/22/15 Pct Recovery = 79% Analysis Date = 06/22/15 Pct Recovery = 79% Analysis Date = 06/17/15 Pct Recovery = 79% Analysis Date = 06/17/15 Pct Recovery = 79% Analysis Date = 06/12/15 Pct Recovery = 78% Analysis Date = 06/12/15 Pct Recovery = 78% Analysis Date = 06/07/15 Pct Recovery = 78% Analysis Date = 06/07/15 Pct Recovery = 78% Analysis Date = 06/02/15 Pct Recovery = 78% Analysis Date = 06/02/15 Pct Recovery = 78% Analysis Date = 05/28/15 Pct Recovery = 78% Analysis Date = 05/28/15 Pct Recovery = 78% Analysis Date = 05/23/15 Pct Recovery = 78% Analysis Date = 05/23/15 Pct Recovery = 78% Analysis Date = 05/18/15 Pct Recovery = 77% Analysis Date = 05/18/15 Pct Recovery = 77% Analysis Date = 05/13/15 Pct Recovery = 77% Analysis Date = 05/13/15 Pct Recovery = 77% Analysis Date = 05/08/15 Pct Recovery = 77% Analysis Date = 05/08/15 Pct Recovery = 77% Analysis Date = 05/03/15 Pct Recovery = 77% Analysis Date = 05/03/15 Pct Recovery = 77% Analysis Date = 04/28/15 Pct Recovery = 76% Analysis Date = 04/28/15 Pct Recovery = 76% Analysis Date = 04/23/15 Pct Recovery = 76% Analysis Date = 04/23/15 Pct Recovery = 76% Analysis Date = 04/18/15 Pct Recovery = 76% Analysis Date = 04/18/15 Pct Recovery = 76% Analysis Date = 04/13/15 Pct Recovery = 76% Analysis Date = 04/13/15 Pct Recovery = 76% Analysis Date = 04/08/15 Pct Recovery = 76% Analysis Date = 04/08/15 Pct Recovery = 76% Analysis Date = 04/03/15 Pct Recovery = 75% Analysis Date = 04/03/15 Pct Recovery = 75% Analysis Date = 03/29/15 Pct Recovery = 75% Analysis Date = 03/29/15 Pct Recovery = 75% Analysis Date = 03/24/15 Pct Recovery = 74% Analysis Date = 03/24/15 Pct Recovery = 74% Analysis Date = 03/19/15 Pct Recovery = 74% Analysis Date = 03/19/15 Pct Recovery = 74% Analysis Date = 03/14/15 Pct Recovery = 74% Analysis Date = 03/14/15 Pct Recovery = 74% Analysis Date = 03/09/15 Pct Recovery = 73% Analysis Date = 03/09/15 Pct Recovery = 73% Analysis Date = 03/04/15 Pct Recovery = 73% Analysis Date = 03/04/15 Pct Recovery = 73% Analysis Date = 02/27/15 Pct Recovery = 72% Analysis Date = 02/27/15 Pct Recovery = 72% Analysis Date = 02/22/15 Pct Recovery = 72% Analysis Date = 02/22/15 Pct Recovery = 72% Analysis Date = 02/17/15 Pct Recovery = 72% Analysis Date = 02/17/15 Pct Recovery = 72% Analysis Date = 02/12/15 Pct Recovery = 71% Analysis Date = 02/12/15 Pct Recovery = 71% Analysis Date = 02/07/15 Pct Recovery = 71% Analysis Date = 02/07/15 Pct Recovery = 71% Analysis Date = 02/02/15 Pct Recovery = 70% Analysis Date = 02/02/15 Pct Recovery = 70% Analysis Date = 01/28/15 Pct Recovery = 70% Analysis Date = 01/28/15 Pct Recovery = 70% Analysis Date = 01/23/15 Pct Recovery = 70% Analysis Date = 01/23/15 Pct Recovery = 70% Analysis Date = 01/18/15 Pct Recovery = 69% Analysis Date = 01/18/15 Pct Recovery = 69% Analysis Date = 01/13/15 Pct Recovery = 69% Analysis Date = 01/13/15 Pct Recovery = 69% Analysis Date = 01/08/15 Pct Recovery = 68% Analysis Date = 01/08/15 Pct Recovery = 68% Analysis Date = 01/03/15 Pct Recovery = 68% Analysis Date = 01/03/15 Pct Recovery = 68% Analysis Date = 12/29/14 Pct Recovery = 67% Analysis Date = 12/29/14 Pct Recovery = 67% Analysis Date = 12/24/14 Pct Recovery = 67% Analysis Date = 12/24/14 Pct Recovery = 67% Analysis Date = 12/19/14 Pct Recovery = 67% Analysis Date = 12/19/14 Pct Recovery = 67% Analysis Date = 12/14/14 Pct Recovery = 66% Analysis Date = 12/14/14 Pct Recovery = 66% Analysis Date = 12/09/14 Pct Recovery = 66% Analysis Date = 12/09/14 Pct Recovery = 66% Analysis Date = 12/04/14 Pct Recovery = 65% Analysis Date = 12/04/14 Pct Recovery = 65% Analysis Date = 11/29/14 Pct Recovery = 65% Analysis Date = 11/29/14 Pct Recovery = 65% Analysis Date = 11/24/14 Pct Recovery = 65% Analysis Date = 11/24/14 Pct Recovery = 65% Analysis Date = 11/19/14 Pct Recovery = 64% Analysis Date = 11/19/14 Pct Recovery = 64% Analysis Date = 11/14/14 Pct Recovery = 64% Analysis Date = 11/14/14 Pct Recovery = 64% Analysis Date = 11/09/14 Pct Recovery = 63% Analysis Date = 11/09/14 Pct Recovery = 63% Analysis Date = 11/04/14 Pct Recovery = 63% Analysis Date = 11/04/14 Pct Recovery = 63% Analysis Date = 10/30/14 Pct Recovery = 62% Analysis Date = 10/30/14 Pct Recovery = 62% Analysis Date = 10/25/14 Pct Recovery = 62% Analysis Date = 10/25/14 Pct Recovery = 62% Analysis Date = 10/20/14 Pct Recovery = 62% Analysis Date = 10/20/14 Pct Recovery = 62% Analysis Date = 10/15/14 Pct Recovery = 61% Analysis Date = 10/15/14 Pct Recovery = 61% Analysis Date = 10/10/14 Pct Recovery = 61% Analysis Date = 10/10/14 Pct Recovery = 61% Analysis Date = 10/05/14 Pct Recovery = 60% Analysis Date = 10/05/14 Pct Recovery = 60% Analysis Date = 09/30/14 Pct Recovery = 60% Analysis Date = 09/30/14 Pct Recovery = 60% Analysis Date = 09/25/14 Pct Recovery = 59% Analysis Date = 09/25/14 Pct Recovery = 59% Analysis Date = 09/20/14 Pct Recovery = 59% Analysis Date = 09/20/14 Pct Recovery = 59% Analysis Date = 09/15/14 Pct Recovery = 59% Analysis Date = 09/15/14 Pct Recovery = 59% Analysis Date = 09/10/14 Pct Recovery = 58% Analysis Date = 09/10/14 Pct Recovery = 58% Analysis Date = 09/05/14 Pct Recovery = 58% Analysis Date = 09/05/14 Pct Recovery = 58% Analysis Date = 08/31/14 Pct Recovery = 57% Analysis Date = 08/31/14 Pct Recovery = 57% Analysis Date = 08/26/14 Pct Recovery = 57% Analysis Date = 08/26/14 Pct Recovery = 57% Analysis Date = 08/21/14 Pct Recovery = 56% Analysis Date = 08/21/14 Pct Recovery = 56% Analysis Date = 08/16/14 Pct Recovery = 56% Analysis Date = 08/16/14 Pct Recovery = 56% Analysis Date = 08/11/14 Pct Recovery = 55% Analysis Date = 08/11/14 Pct Recovery = 55% Analysis Date = 08/06/14 Pct Recovery = 55% Analysis Date = 08/06/14 Pct Recovery = 55% Analysis Date = 08/01/14 Pct Recovery = 55% Analysis Date = 08/01/14 Pct Recovery = 55% Analysis Date = 07/27/14 Pct Recovery = 54% Analysis Date = 07/27/14 Pct Recovery = 54% Analysis Date = 07/22/14 Pct Recovery = 54% Analysis Date = 07/22/14 Pct Recovery = 54% Analysis Date = 07/17/14 Pct Recovery = 53% Analysis Date = 07/17/14 Pct Recovery = 53% Analysis Date = 07/12/14 Pct Recovery = 53% Analysis Date = 07/12/14 Pct Recovery = 53% Analysis Date = 07/07/14 Pct Recovery = 52% Analysis Date = 07/07/14 Pct Recovery = 52% Analysis Date = 07/02/14 Pct Recovery = 52% Analysis Date = 07/02/14 Pct Recovery = 52% Analysis Date = 06/27/14 Pct Recovery = 51% Analysis Date = 06/27/14 Pct Recovery = 51% Analysis Date = 06/22/14 Pct Recovery = 51% Analysis Date = 06/22/14 Pct Recovery = 51% Analysis Date = 06/17/14 Pct Recovery = 50% Analysis Date = 06/17/14 Pct Recovery = 50% Analysis Date = 06/12/14 Pct Recovery = 50% Analysis Date = 06/12/14 Pct Recovery = 50% Analysis Date = 06/07/14 Pct Recovery = 49% Analysis Date = 06/07/14 Pct Recovery = 49% Analysis Date = 06/02/14 Pct Recovery = 49% Analysis Date = 06/02/14 Pct Recovery = 49% Analysis Date = 05/28/14 Pct Recovery = 48% Analysis Date = 05/28/14 Pct Recovery = 48% Analysis Date = 05/23/14 Pct Recovery = 48% Analysis Date = 05/23/14 Pct Recovery = 48% Analysis Date = 05/18/14 Pct Recovery = 48% Analysis Date = 05/18/14 Pct Recovery = 48% Analysis Date = 05/13/14 Pct Recovery = 47% Analysis Date = 05/13/14 Pct Recovery = 47% Analysis Date = 05/08/14 Pct Recovery = 47% Analysis Date = 05/08/14 Pct Recovery = 47% Analysis Date = 05/03/14 Pct Recovery = 46% Analysis Date = 05/03/14 Pct Recovery = 46% Analysis Date = 04/28/14 Pct Recovery = 46% Analysis Date = 04/28/14 Pct Recovery = 46% Analysis Date = 04/23/14 Pct Recovery = 45% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
PENTOXIFYLLINE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 2 50% 3% 50% 3%
>= Reporting Level 66 72% 13% 74% 12%
Total 68 71% 14% 74% 13%

Sample Statistics
PENTOXIFYLLINE

Characteristic N % % Basis
Plotted 68 88% Spiked
Estimated Values 10 13% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 3 4% Spiked
Spiked 77 .  
False Negatives 6 8% 6 out of 77
Not Spiked 38 .  
False Positives 0 0% 0 out of 38

BQS OBSP Determination:
PHENAZOPYRIDINE
METHOD: 2440 , TESTIDCODE: 68008LCM56
Open Data Set

Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 57% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 60% Analysis Date = 01/17/16 SpikeMix = ERA 0406-15-09: 80 µl & ERA 0406-15-07A: 80 µl Pct Recovery = 65% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 80 µl & Abs 051315: 80 µl Pct Recovery = 66% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 80 µl & ERA 0406-15-08: 80 µl Pct Recovery = 72% Analysis Date = 11/04/15 SpikeMix = Abs 052215: 80 µl & Abs 050115: 80 µl Pct Recovery = 67% Analysis Date = 11/18/16 SpikeMix = ERA 04281604: 80 µl & ERA 04281603: 80 µl Pct Recovery = 60% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & ERA 04281604: 80 µl Pct Recovery = 60% Analysis Date = 09/24/16 SpikeMix = Crescent EN160610015: 80 µl & Abs 061416: 80 µl Pct Recovery = 89% Analysis Date = 09/24/16 SpikeMix = Abs 061416: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 92% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 88% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 95% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 81% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 80% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-04: 15 µl & Abs 041814: 15 µl Pct Recovery = 111% Analysis Date = 12/06/14 SpikeMix = ERA 0318-14-02: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 85% Analysis Date = 10/25/14 SpikeMix = Abs 041614: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 79% Analysis Date = 10/11/14 SpikeMix = ERA 0318-14-02: 60 µl & ERA 0319-14-04: 60 µl Pct Recovery = 75% Analysis Date = 08/28/14 SpikeMix = ERA 0319-14-04: 60 µl & ERA 0319-14-05: 60 µl Pct Recovery = 86% Analysis Date = 05/07/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 116% Analysis Date = 03/11/15 SpikeMix = ERA 0318-14-02: 15 µl & Abs 041714: 15 µl Pct Recovery = 119% Analysis Date = 01/16/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 110% Analysis Date = 12/06/14 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 77% Analysis Date = 08/21/14 SpikeMix = ERA 0318-14-02: 60 µl & Abs 041714: 60 µl Pct Recovery = 69% Analysis Date = 07/12/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 76% Analysis Date = 06/11/14 SpikeMix = Abs 041614: 60 µl & Abs 041714: 60 µl Pct Recovery = 81% Analysis Date = 05/21/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 79% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-07A: 40 µl & Abs 051315: 40 µl Pct Recovery = 55% Analysis Date = 11/04/15 SpikeMix = ERA 0406-15-07A: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 58% Analysis Date = 09/10/15 SpikeMix = Abs 052215: 40 µl & ERA 0406-15-07A: 40 µl Pct Recovery = 58% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 72% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 64% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 64% Analysis Date = 02/23/16 SpikeMix = Abs 052215: 40 µl & Abs 050115: 40 µl Pct Recovery = 66% Analysis Date = 07/31/15 SpikeMix = ERA 0406-15-09: 40 µl & Abs 050115: 40 µl Pct Recovery = 72% Analysis Date = 07/30/15 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 68% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 81% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 95% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 73% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 73% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 53% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 61% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 105% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 93% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 75% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 74% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 104% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 114% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 105% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 100% Analysis Date = 04/30/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 124% Analysis Date = 04/10/15 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 118% Analysis Date = 02/10/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 100% Analysis Date = 12/07/14 SpikeMix = ERA 0318-14-02: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 85% Analysis Date = 10/11/14 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 88% Analysis Date = 11/04/14 SpikeMix = Abs 041714: 8 µl & ERA 0319-14-05: 8 µl Pct Recovery = 90% Analysis Date = 04/23/14 SpikeMix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.2: 20 µl Pct Recovery = 82% Analysis Date = 09/12/14 SpikeMix = Abs 041614: 30 µl & ERA 0319-14-04: 30 µl Pct Recovery = 74% Analysis Date = 08/16/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 74% Analysis Date = 07/13/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 83% Analysis Date = 10/10/14 SpikeMix = Abs 041714: 30 µl & Abs 041814: 30 µl Pct Recovery = 87% Analysis Date = 07/20/14 SpikeMix = ERA 0318-14-02: 30 µl & Abs 041714: 30 µl Pct Recovery = 53% Analysis Date = 06/28/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 81% Analysis Date = 05/17/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 74% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 80% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 67% Analysis Date = 04/27/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 94% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 39% Analysis Date = 11/24/15 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 53% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-09: 20 µl Pct Recovery = 79% Analysis Date = 09/15/15 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 74% Analysis Date = 11/25/15 SpikeMix = Abs 050115: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 44% Analysis Date = 11/24/15 SpikeMix = ERA 0406-15-09: 20 µl & Abs 050115: 20 µl Pct Recovery = 59% Analysis Date = 08/27/15 SpikeMix = Abs 052215: 20 µl & Abs 050115: 20 µl Pct Recovery = 71% Analysis Date = 08/11/15 SpikeMix = Abs 050115: 20 µl & Abs 051315: 20 µl Pct Recovery = 46% Analysis Date = 07/09/15 SpikeMix = Abs 050115: 20 µl & Abs 052215: 20 µl Pct Recovery = 64% Analysis Date = 06/09/15 SpikeMix = Abs 051315: 20 µl & Abs 050115: 20 µl Pct Recovery = 77% Analysis Date = 01/04/17 Pct Recovery = 85% Analysis Date = 12/31/16 Pct Recovery = 84% Analysis Date = 12/31/16 Pct Recovery = 84% Analysis Date = 12/26/16 Pct Recovery = 84% Analysis Date = 12/26/16 Pct Recovery = 84% Analysis Date = 12/21/16 Pct Recovery = 84% Analysis Date = 12/21/16 Pct Recovery = 84% Analysis Date = 12/16/16 Pct Recovery = 84% Analysis Date = 12/16/16 Pct Recovery = 84% Analysis Date = 12/11/16 Pct Recovery = 84% Analysis Date = 12/11/16 Pct Recovery = 84% Analysis Date = 12/06/16 Pct Recovery = 83% Analysis Date = 12/06/16 Pct Recovery = 83% Analysis Date = 12/01/16 Pct Recovery = 83% Analysis Date = 12/01/16 Pct Recovery = 83% Analysis Date = 11/26/16 Pct Recovery = 83% Analysis Date = 11/26/16 Pct Recovery = 83% Analysis Date = 11/21/16 Pct Recovery = 83% Analysis Date = 11/21/16 Pct Recovery = 83% Analysis Date = 11/16/16 Pct Recovery = 83% Analysis Date = 11/16/16 Pct Recovery = 83% Analysis Date = 11/11/16 Pct Recovery = 83% Analysis Date = 11/11/16 Pct Recovery = 83% Analysis Date = 11/06/16 Pct Recovery = 82% Analysis Date = 11/06/16 Pct Recovery = 82% Analysis Date = 11/01/16 Pct Recovery = 82% Analysis Date = 11/01/16 Pct Recovery = 82% Analysis Date = 10/27/16 Pct Recovery = 82% Analysis Date = 10/27/16 Pct Recovery = 82% Analysis Date = 10/22/16 Pct Recovery = 82% Analysis Date = 10/22/16 Pct Recovery = 82% Analysis Date = 10/17/16 Pct Recovery = 82% Analysis Date = 10/17/16 Pct Recovery = 82% Analysis Date = 10/13/16 Pct Recovery = 81% Analysis Date = 10/13/16 Pct Recovery = 81% Analysis Date = 10/08/16 Pct Recovery = 81% Analysis Date = 10/08/16 Pct Recovery = 81% Analysis Date = 10/03/16 Pct Recovery = 81% Analysis Date = 10/03/16 Pct Recovery = 81% Analysis Date = 09/28/16 Pct Recovery = 81% Analysis Date = 09/28/16 Pct Recovery = 81% Analysis Date = 09/23/16 Pct Recovery = 80% Analysis Date = 09/23/16 Pct Recovery = 80% Analysis Date = 09/18/16 Pct Recovery = 80% Analysis Date = 09/18/16 Pct Recovery = 80% Analysis Date = 09/13/16 Pct Recovery = 80% Analysis Date = 09/13/16 Pct Recovery = 80% Analysis Date = 09/08/16 Pct Recovery = 80% Analysis Date = 09/08/16 Pct Recovery = 80% Analysis Date = 09/03/16 Pct Recovery = 79% Analysis Date = 09/03/16 Pct Recovery = 79% Analysis Date = 08/29/16 Pct Recovery = 79% Analysis Date = 08/29/16 Pct Recovery = 79% Analysis Date = 08/24/16 Pct Recovery = 79% Analysis Date = 08/24/16 Pct Recovery = 79% Analysis Date = 08/19/16 Pct Recovery = 79% Analysis Date = 08/19/16 Pct Recovery = 79% Analysis Date = 08/14/16 Pct Recovery = 78% Analysis Date = 08/14/16 Pct Recovery = 78% Analysis Date = 08/09/16 Pct Recovery = 78% Analysis Date = 08/09/16 Pct Recovery = 78% Analysis Date = 08/04/16 Pct Recovery = 78% Analysis Date = 08/04/16 Pct Recovery = 78% Analysis Date = 07/30/16 Pct Recovery = 78% Analysis Date = 07/30/16 Pct Recovery = 78% Analysis Date = 07/25/16 Pct Recovery = 77% Analysis Date = 07/25/16 Pct Recovery = 77% Analysis Date = 07/21/16 Pct Recovery = 77% Analysis Date = 07/21/16 Pct Recovery = 77% Analysis Date = 07/16/16 Pct Recovery = 77% Analysis Date = 07/16/16 Pct Recovery = 77% Analysis Date = 07/11/16 Pct Recovery = 77% Analysis Date = 07/11/16 Pct Recovery = 77% Analysis Date = 07/06/16 Pct Recovery = 76% Analysis Date = 07/06/16 Pct Recovery = 76% Analysis Date = 07/01/16 Pct Recovery = 76% Analysis Date = 07/01/16 Pct Recovery = 76% Analysis Date = 06/26/16 Pct Recovery = 76% Analysis Date = 06/26/16 Pct Recovery = 76% Analysis Date = 06/21/16 Pct Recovery = 76% Analysis Date = 06/21/16 Pct Recovery = 76% Analysis Date = 06/16/16 Pct Recovery = 75% Analysis Date = 06/16/16 Pct Recovery = 75% Analysis Date = 06/11/16 Pct Recovery = 75% Analysis Date = 06/11/16 Pct Recovery = 75% Analysis Date = 06/06/16 Pct Recovery = 75% Analysis Date = 06/06/16 Pct Recovery = 75% Analysis Date = 06/01/16 Pct Recovery = 75% Analysis Date = 06/01/16 Pct Recovery = 75% Analysis Date = 05/27/16 Pct Recovery = 74% Analysis Date = 05/27/16 Pct Recovery = 74% Analysis Date = 05/22/16 Pct Recovery = 74% Analysis Date = 05/22/16 Pct Recovery = 74% Analysis Date = 05/17/16 Pct Recovery = 74% Analysis Date = 05/17/16 Pct Recovery = 74% Analysis Date = 05/12/16 Pct Recovery = 74% Analysis Date = 05/12/16 Pct Recovery = 74% Analysis Date = 05/07/16 Pct Recovery = 73% Analysis Date = 05/07/16 Pct Recovery = 73% Analysis Date = 05/02/16 Pct Recovery = 73% Analysis Date = 05/02/16 Pct Recovery = 73% Analysis Date = 04/28/16 Pct Recovery = 73% Analysis Date = 04/28/16 Pct Recovery = 73% Analysis Date = 04/23/16 Pct Recovery = 72% Analysis Date = 04/23/16 Pct Recovery = 72% Analysis Date = 04/18/16 Pct Recovery = 72% Analysis Date = 04/18/16 Pct Recovery = 72% Analysis Date = 04/13/16 Pct Recovery = 72% Analysis Date = 04/13/16 Pct Recovery = 72% Analysis Date = 04/08/16 Pct Recovery = 72% Analysis Date = 04/08/16 Pct Recovery = 72% Analysis Date = 04/03/16 Pct Recovery = 71% Analysis Date = 04/03/16 Pct Recovery = 71% Analysis Date = 03/29/16 Pct Recovery = 71% Analysis Date = 03/29/16 Pct Recovery = 71% Analysis Date = 03/24/16 Pct Recovery = 71% Analysis Date = 03/24/16 Pct Recovery = 71% Analysis Date = 03/19/16 Pct Recovery = 71% Analysis Date = 03/19/16 Pct Recovery = 71% Analysis Date = 03/14/16 Pct Recovery = 71% Analysis Date = 03/14/16 Pct Recovery = 71% Analysis Date = 03/09/16 Pct Recovery = 70% Analysis Date = 03/09/16 Pct Recovery = 70% Analysis Date = 03/04/16 Pct Recovery = 70% Analysis Date = 03/04/16 Pct Recovery = 70% Analysis Date = 02/28/16 Pct Recovery = 70% Analysis Date = 02/28/16 Pct Recovery = 70% Analysis Date = 02/23/16 Pct Recovery = 70% Analysis Date = 02/23/16 Pct Recovery = 70% Analysis Date = 02/18/16 Pct Recovery = 69% Analysis Date = 02/18/16 Pct Recovery = 69% Analysis Date = 02/13/16 Pct Recovery = 69% Analysis Date = 02/13/16 Pct Recovery = 69% Analysis Date = 02/09/16 Pct Recovery = 69% Analysis Date = 02/09/16 Pct Recovery = 69% Analysis Date = 02/04/16 Pct Recovery = 69% Analysis Date = 02/04/16 Pct Recovery = 69% Analysis Date = 01/30/16 Pct Recovery = 68% Analysis Date = 01/30/16 Pct Recovery = 68% Analysis Date = 01/25/16 Pct Recovery = 68% Analysis Date = 01/25/16 Pct Recovery = 68% Analysis Date = 01/20/16 Pct Recovery = 68% Analysis Date = 01/20/16 Pct Recovery = 68% Analysis Date = 01/15/16 Pct Recovery = 68% Analysis Date = 01/15/16 Pct Recovery = 68% Analysis Date = 01/10/16 Pct Recovery = 68% Analysis Date = 01/10/16 Pct Recovery = 68% Analysis Date = 01/05/16 Pct Recovery = 68% Analysis Date = 01/05/16 Pct Recovery = 68% Analysis Date = 12/31/15 Pct Recovery = 68% Analysis Date = 12/31/15 Pct Recovery = 68% Analysis Date = 12/26/15 Pct Recovery = 68% Analysis Date = 12/26/15 Pct Recovery = 68% Analysis Date = 12/21/15 Pct Recovery = 68% Analysis Date = 12/21/15 Pct Recovery = 68% Analysis Date = 12/16/15 Pct Recovery = 68% Analysis Date = 12/16/15 Pct Recovery = 68% Analysis Date = 12/11/15 Pct Recovery = 68% Analysis Date = 12/11/15 Pct Recovery = 68% Analysis Date = 12/06/15 Pct Recovery = 69% Analysis Date = 12/06/15 Pct Recovery = 69% Analysis Date = 12/01/15 Pct Recovery = 69% Analysis Date = 12/01/15 Pct Recovery = 69% Analysis Date = 11/26/15 Pct Recovery = 69% Analysis Date = 11/26/15 Pct Recovery = 69% Analysis Date = 11/21/15 Pct Recovery = 69% Analysis Date = 11/21/15 Pct Recovery = 69% Analysis Date = 11/17/15 Pct Recovery = 69% Analysis Date = 11/17/15 Pct Recovery = 69% Analysis Date = 11/12/15 Pct Recovery = 69% Analysis Date = 11/12/15 Pct Recovery = 69% Analysis Date = 11/07/15 Pct Recovery = 69% Analysis Date = 11/07/15 Pct Recovery = 69% Analysis Date = 11/02/15 Pct Recovery = 69% Analysis Date = 11/02/15 Pct Recovery = 69% Analysis Date = 10/28/15 Pct Recovery = 70% Analysis Date = 10/28/15 Pct Recovery = 70% Analysis Date = 10/23/15 Pct Recovery = 70% Analysis Date = 10/23/15 Pct Recovery = 70% Analysis Date = 10/18/15 Pct Recovery = 71% Analysis Date = 10/18/15 Pct Recovery = 71% Analysis Date = 10/13/15 Pct Recovery = 71% Analysis Date = 10/13/15 Pct Recovery = 71% Analysis Date = 10/08/15 Pct Recovery = 72% Analysis Date = 10/08/15 Pct Recovery = 72% Analysis Date = 10/03/15 Pct Recovery = 72% Analysis Date = 10/03/15 Pct Recovery = 72% Analysis Date = 09/28/15 Pct Recovery = 72% Analysis Date = 09/28/15 Pct Recovery = 72% Analysis Date = 09/23/15 Pct Recovery = 73% Analysis Date = 09/23/15 Pct Recovery = 73% Analysis Date = 09/18/15 Pct Recovery = 73% Analysis Date = 09/18/15 Pct Recovery = 73% Analysis Date = 09/13/15 Pct Recovery = 74% Analysis Date = 09/13/15 Pct Recovery = 74% Analysis Date = 09/08/15 Pct Recovery = 74% Analysis Date = 09/08/15 Pct Recovery = 74% Analysis Date = 09/03/15 Pct Recovery = 75% Analysis Date = 09/03/15 Pct Recovery = 75% Analysis Date = 08/29/15 Pct Recovery = 75% Analysis Date = 08/29/15 Pct Recovery = 75% Analysis Date = 08/25/15 Pct Recovery = 76% Analysis Date = 08/25/15 Pct Recovery = 76% Analysis Date = 08/20/15 Pct Recovery = 76% Analysis Date = 08/20/15 Pct Recovery = 76% Analysis Date = 08/15/15 Pct Recovery = 76% Analysis Date = 08/15/15 Pct Recovery = 76% Analysis Date = 08/10/15 Pct Recovery = 77% Analysis Date = 08/10/15 Pct Recovery = 77% Analysis Date = 08/05/15 Pct Recovery = 77% Analysis Date = 08/05/15 Pct Recovery = 77% Analysis Date = 07/31/15 Pct Recovery = 78% Analysis Date = 07/31/15 Pct Recovery = 78% Analysis Date = 07/26/15 Pct Recovery = 78% Analysis Date = 07/26/15 Pct Recovery = 78% Analysis Date = 07/21/15 Pct Recovery = 78% Analysis Date = 07/21/15 Pct Recovery = 78% Analysis Date = 07/16/15 Pct Recovery = 79% Analysis Date = 07/16/15 Pct Recovery = 79% Analysis Date = 07/11/15 Pct Recovery = 79% Analysis Date = 07/11/15 Pct Recovery = 79% Analysis Date = 07/06/15 Pct Recovery = 79% Analysis Date = 07/06/15 Pct Recovery = 79% Analysis Date = 07/01/15 Pct Recovery = 79% Analysis Date = 07/01/15 Pct Recovery = 79% Analysis Date = 06/26/15 Pct Recovery = 80% Analysis Date = 06/26/15 Pct Recovery = 80% Analysis Date = 06/21/15 Pct Recovery = 80% Analysis Date = 06/21/15 Pct Recovery = 80% Analysis Date = 06/16/15 Pct Recovery = 80% Analysis Date = 06/16/15 Pct Recovery = 80% Analysis Date = 06/11/15 Pct Recovery = 81% Analysis Date = 06/11/15 Pct Recovery = 81% Analysis Date = 06/07/15 Pct Recovery = 81% Analysis Date = 06/07/15 Pct Recovery = 81% Analysis Date = 06/02/15 Pct Recovery = 81% Analysis Date = 06/02/15 Pct Recovery = 81% Analysis Date = 05/28/15 Pct Recovery = 81% Analysis Date = 05/28/15 Pct Recovery = 81% Analysis Date = 05/23/15 Pct Recovery = 82% Analysis Date = 05/23/15 Pct Recovery = 82% Analysis Date = 05/18/15 Pct Recovery = 82% Analysis Date = 05/18/15 Pct Recovery = 82% Analysis Date = 05/13/15 Pct Recovery = 82% Analysis Date = 05/13/15 Pct Recovery = 82% Analysis Date = 05/08/15 Pct Recovery = 83% Analysis Date = 05/08/15 Pct Recovery = 83% Analysis Date = 05/03/15 Pct Recovery = 83% Analysis Date = 05/03/15 Pct Recovery = 83% Analysis Date = 04/28/15 Pct Recovery = 83% Analysis Date = 04/28/15 Pct Recovery = 83% Analysis Date = 04/23/15 Pct Recovery = 84% Analysis Date = 04/23/15 Pct Recovery = 84% Analysis Date = 04/18/15 Pct Recovery = 84% Analysis Date = 04/18/15 Pct Recovery = 84% Analysis Date = 04/13/15 Pct Recovery = 84% Analysis Date = 04/13/15 Pct Recovery = 84% Analysis Date = 04/08/15 Pct Recovery = 84% Analysis Date = 04/08/15 Pct Recovery = 84% Analysis Date = 04/03/15 Pct Recovery = 84% Analysis Date = 04/03/15 Pct Recovery = 84% Analysis Date = 03/29/15 Pct Recovery = 84% Analysis Date = 03/29/15 Pct Recovery = 84% Analysis Date = 03/24/15 Pct Recovery = 84% Analysis Date = 03/24/15 Pct Recovery = 84% Analysis Date = 03/19/15 Pct Recovery = 84% Analysis Date = 03/19/15 Pct Recovery = 84% Analysis Date = 03/15/15 Pct Recovery = 84% Analysis Date = 03/15/15 Pct Recovery = 84% Analysis Date = 03/10/15 Pct Recovery = 84% Analysis Date = 03/10/15 Pct Recovery = 84% Analysis Date = 03/05/15 Pct Recovery = 84% Analysis Date = 03/05/15 Pct Recovery = 84% Analysis Date = 02/28/15 Pct Recovery = 84% Analysis Date = 02/28/15 Pct Recovery = 84% Analysis Date = 02/23/15 Pct Recovery = 84% Analysis Date = 02/23/15 Pct Recovery = 84% Analysis Date = 02/18/15 Pct Recovery = 84% Analysis Date = 02/18/15 Pct Recovery = 84% Analysis Date = 02/13/15 Pct Recovery = 84% Analysis Date = 02/13/15 Pct Recovery = 84% Analysis Date = 02/08/15 Pct Recovery = 84% Analysis Date = 02/08/15 Pct Recovery = 84% Analysis Date = 02/03/15 Pct Recovery = 84% Analysis Date = 02/03/15 Pct Recovery = 84% Analysis Date = 01/29/15 Pct Recovery = 84% Analysis Date = 01/29/15 Pct Recovery = 84% Analysis Date = 01/24/15 Pct Recovery = 84% Analysis Date = 01/24/15 Pct Recovery = 84% Analysis Date = 01/19/15 Pct Recovery = 84% Analysis Date = 01/19/15 Pct Recovery = 84% Analysis Date = 01/14/15 Pct Recovery = 84% Analysis Date = 01/14/15 Pct Recovery = 84% Analysis Date = 01/09/15 Pct Recovery = 84% Analysis Date = 01/09/15 Pct Recovery = 84% Analysis Date = 01/04/15 Pct Recovery = 84% Analysis Date = 01/04/15 Pct Recovery = 84% Analysis Date = 12/30/14 Pct Recovery = 84% Analysis Date = 12/30/14 Pct Recovery = 84% Analysis Date = 12/25/14 Pct Recovery = 84% Analysis Date = 12/25/14 Pct Recovery = 84% Analysis Date = 12/21/14 Pct Recovery = 84% Analysis Date = 12/21/14 Pct Recovery = 84% Analysis Date = 12/16/14 Pct Recovery = 84% Analysis Date = 12/16/14 Pct Recovery = 84% Analysis Date = 12/11/14 Pct Recovery = 84% Analysis Date = 12/11/14 Pct Recovery = 84% Analysis Date = 12/06/14 Pct Recovery = 84% Analysis Date = 12/06/14 Pct Recovery = 84% Analysis Date = 12/01/14 Pct Recovery = 84% Analysis Date = 12/01/14 Pct Recovery = 84% Analysis Date = 11/26/14 Pct Recovery = 84% Analysis Date = 11/26/14 Pct Recovery = 84% Analysis Date = 11/21/14 Pct Recovery = 84% Analysis Date = 11/21/14 Pct Recovery = 84% Analysis Date = 11/16/14 Pct Recovery = 84% Analysis Date = 11/16/14 Pct Recovery = 84% Analysis Date = 11/11/14 Pct Recovery = 83% Analysis Date = 11/11/14 Pct Recovery = 83% Analysis Date = 11/06/14 Pct Recovery = 83% Analysis Date = 11/06/14 Pct Recovery = 83% Analysis Date = 11/01/14 Pct Recovery = 83% Analysis Date = 11/01/14 Pct Recovery = 83% Analysis Date = 10/27/14 Pct Recovery = 83% Analysis Date = 10/27/14 Pct Recovery = 83% Analysis Date = 10/22/14 Pct Recovery = 83% Analysis Date = 10/22/14 Pct Recovery = 83% Analysis Date = 10/17/14 Pct Recovery = 83% Analysis Date = 10/17/14 Pct Recovery = 83% Analysis Date = 10/12/14 Pct Recovery = 83% Analysis Date = 10/12/14 Pct Recovery = 83% Analysis Date = 10/07/14 Pct Recovery = 83% Analysis Date = 10/07/14 Pct Recovery = 83% Analysis Date = 10/03/14 Pct Recovery = 83% Analysis Date = 10/03/14 Pct Recovery = 83% Analysis Date = 09/28/14 Pct Recovery = 83% Analysis Date = 09/28/14 Pct Recovery = 83% Analysis Date = 09/23/14 Pct Recovery = 83% Analysis Date = 09/23/14 Pct Recovery = 83% Analysis Date = 09/18/14 Pct Recovery = 83% Analysis Date = 09/18/14 Pct Recovery = 83% Analysis Date = 09/13/14 Pct Recovery = 83% Analysis Date = 09/13/14 Pct Recovery = 83% Analysis Date = 09/08/14 Pct Recovery = 82% Analysis Date = 09/08/14 Pct Recovery = 82% Analysis Date = 09/03/14 Pct Recovery = 82% Analysis Date = 09/03/14 Pct Recovery = 82% Analysis Date = 08/29/14 Pct Recovery = 82% Analysis Date = 08/29/14 Pct Recovery = 82% Analysis Date = 08/24/14 Pct Recovery = 82% Analysis Date = 08/24/14 Pct Recovery = 82% Analysis Date = 08/19/14 Pct Recovery = 82% Analysis Date = 08/19/14 Pct Recovery = 82% Analysis Date = 08/14/14 Pct Recovery = 82% Analysis Date = 08/14/14 Pct Recovery = 82% Analysis Date = 08/09/14 Pct Recovery = 82% Analysis Date = 08/09/14 Pct Recovery = 82% Analysis Date = 08/04/14 Pct Recovery = 82% Analysis Date = 08/04/14 Pct Recovery = 82% Analysis Date = 07/30/14 Pct Recovery = 81% Analysis Date = 07/30/14 Pct Recovery = 81% Analysis Date = 07/25/14 Pct Recovery = 81% Analysis Date = 07/25/14 Pct Recovery = 81% Analysis Date = 07/20/14 Pct Recovery = 81% Analysis Date = 07/20/14 Pct Recovery = 81% Analysis Date = 07/15/14 Pct Recovery = 81% Analysis Date = 07/15/14 Pct Recovery = 81% Analysis Date = 07/11/14 Pct Recovery = 81% Analysis Date = 07/11/14 Pct Recovery = 81% Analysis Date = 07/06/14 Pct Recovery = 81% Analysis Date = 07/06/14 Pct Recovery = 81% Analysis Date = 07/01/14 Pct Recovery = 81% Analysis Date = 07/01/14 Pct Recovery = 81% Analysis Date = 06/26/14 Pct Recovery = 80% Analysis Date = 06/26/14 Pct Recovery = 80% Analysis Date = 06/21/14 Pct Recovery = 80% Analysis Date = 06/21/14 Pct Recovery = 80% Analysis Date = 06/16/14 Pct Recovery = 80% Analysis Date = 06/16/14 Pct Recovery = 80% Analysis Date = 06/11/14 Pct Recovery = 80% Analysis Date = 06/11/14 Pct Recovery = 80% Analysis Date = 06/06/14 Pct Recovery = 80% Analysis Date = 06/06/14 Pct Recovery = 80% Analysis Date = 06/01/14 Pct Recovery = 79% Analysis Date = 06/01/14 Pct Recovery = 79% Analysis Date = 05/27/14 Pct Recovery = 79% Analysis Date = 05/27/14 Pct Recovery = 79% Analysis Date = 05/22/14 Pct Recovery = 79% Analysis Date = 05/22/14 Pct Recovery = 79% Analysis Date = 05/17/14 Pct Recovery = 79% Analysis Date = 05/17/14 Pct Recovery = 79% Analysis Date = 05/12/14 Pct Recovery = 79% Analysis Date = 05/12/14 Pct Recovery = 79% Analysis Date = 05/07/14 Pct Recovery = 79% Analysis Date = 05/07/14 Pct Recovery = 79% Analysis Date = 05/02/14 Pct Recovery = 78% Analysis Date = 05/02/14 Pct Recovery = 78% Analysis Date = 04/27/14 Pct Recovery = 78% Analysis Date = 04/27/14 Pct Recovery = 78% Analysis Date = 04/23/14 Pct Recovery = 78% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
PHENAZOPYRIDINE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 77 78% 19% 76% 17%
Total 77 78% 19% 76% 17%

Sample Statistics
PHENAZOPYRIDINE

Characteristic N % % Basis
Plotted 77 97% Spiked
Estimated Values 21 27% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 2 3% Spiked
Spiked 79 .  
False Negatives 0 0% 0 out of 79
Not Spiked 36 .  
False Positives 0 0% 0 out of 36

BQS OBSP Determination:
PHENDIMETRAZINE
METHOD: 2440 , TESTIDCODE: 67496LCM56
Open Data Set

The SGPlot Procedure

Sample Statistics
PHENDIMETRAZINE

Characteristic N % % Basis
Plotted 0 . Spiked
Estimated Values 0 . Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 . Spiked
Spiked 0 .  
False Negatives 0 . 0 out of 0
Not Spiked 115 .  
False Positives 0 0% 0 out of 115

BQS OBSP Determination:
PHENYTOIN
METHOD: 2440 , TESTIDCODE: 67466LCM56
Open Data Set

Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 94% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 114% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 80 µl & ERA 0406-15-08: 80 µl Pct Recovery = 95% Analysis Date = 11/04/15 SpikeMix = Abs 052215: 80 µl & Abs 050115: 80 µl Pct Recovery = 96% Analysis Date = 01/17/16 SpikeMix = ERA 0406-15-09: 80 µl & ERA 0406-15-07A: 80 µl Pct Recovery = 80% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 80 µl & Abs 051315: 80 µl Pct Recovery = 73% Analysis Date = 11/18/16 SpikeMix = ERA 04281604: 80 µl & ERA 04281603: 80 µl Pct Recovery = 81% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & ERA 04281604: 80 µl Pct Recovery = 80% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 72% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 76% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 83% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 86% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 102% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 100% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-04: 15 µl & Abs 041814: 15 µl Pct Recovery = 81% Analysis Date = 12/06/14 SpikeMix = ERA 0318-14-02: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 88% Analysis Date = 10/25/14 SpikeMix = Abs 041614: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 88% Analysis Date = 10/11/14 SpikeMix = ERA 0318-14-02: 60 µl & ERA 0319-14-04: 60 µl Pct Recovery = 81% Analysis Date = 08/28/14 SpikeMix = ERA 0319-14-04: 60 µl & ERA 0319-14-05: 60 µl Pct Recovery = 83% Analysis Date = 05/07/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 93% Analysis Date = 03/11/15 SpikeMix = ERA 0318-14-02: 15 µl & Abs 041714: 15 µl Pct Recovery = 95% Analysis Date = 01/16/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 93% Analysis Date = 12/06/14 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 68% Analysis Date = 08/21/14 SpikeMix = ERA 0318-14-02: 60 µl & Abs 041714: 60 µl Pct Recovery = 74% Analysis Date = 07/12/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 88% Analysis Date = 06/11/14 SpikeMix = Abs 041614: 60 µl & Abs 041714: 60 µl Pct Recovery = 93% Analysis Date = 05/21/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 83% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 94% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 76% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 90% Analysis Date = 02/23/16 SpikeMix = Abs 052215: 40 µl & Abs 050115: 40 µl Pct Recovery = 79% Analysis Date = 07/31/15 SpikeMix = ERA 0406-15-09: 40 µl & Abs 050115: 40 µl Pct Recovery = 82% Analysis Date = 07/30/15 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 71% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-07A: 40 µl & Abs 051315: 40 µl Pct Recovery = 78% Analysis Date = 11/04/15 SpikeMix = ERA 0406-15-07A: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 89% Analysis Date = 09/10/15 SpikeMix = Abs 052215: 40 µl & ERA 0406-15-07A: 40 µl Pct Recovery = 86% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 72% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 83% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 78% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 74% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 115% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 124% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 91% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 93% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 95% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 88% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 69% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 77% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 75% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 79% Analysis Date = 04/30/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 110% Analysis Date = 04/10/15 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 91% Analysis Date = 02/10/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 98% Analysis Date = 12/07/14 SpikeMix = ERA 0318-14-02: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 85% Analysis Date = 10/11/14 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 79% Analysis Date = 11/04/14 SpikeMix = Abs 041714: 8 µl & ERA 0319-14-05: 8 µl Pct Recovery = 81% Analysis Date = 09/12/14 SpikeMix = Abs 041614: 30 µl & ERA 0319-14-04: 30 µl Pct Recovery = 80% Analysis Date = 08/16/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 64% Analysis Date = 07/13/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 77% Analysis Date = 10/10/14 SpikeMix = Abs 041714: 30 µl & Abs 041814: 30 µl Pct Recovery = 93% Analysis Date = 07/20/14 SpikeMix = ERA 0318-14-02: 30 µl & Abs 041714: 30 µl Pct Recovery = 76% Analysis Date = 06/28/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 72% Analysis Date = 05/17/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 99% Analysis Date = 11/25/15 SpikeMix = Abs 050115: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 99% Analysis Date = 11/24/15 SpikeMix = ERA 0406-15-09: 20 µl & Abs 050115: 20 µl Pct Recovery = 94% Analysis Date = 08/27/15 SpikeMix = Abs 052215: 20 µl & Abs 050115: 20 µl Pct Recovery = 95% Analysis Date = 08/11/15 SpikeMix = Abs 050115: 20 µl & Abs 051315: 20 µl Pct Recovery = 79% Analysis Date = 07/09/15 SpikeMix = Abs 050115: 20 µl & Abs 052215: 20 µl Pct Recovery = 82% Analysis Date = 06/09/15 SpikeMix = Abs 051315: 20 µl & Abs 050115: 20 µl Pct Recovery = 79% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 77% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 80% Analysis Date = 04/27/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 120% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 109% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 93% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 61% Analysis Date = 11/24/15 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 96% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-09: 20 µl Pct Recovery = 48% Analysis Date = 01/18/17 Pct Recovery = 91% Analysis Date = 01/14/17 Pct Recovery = 91% Analysis Date = 01/14/17 Pct Recovery = 91% Analysis Date = 01/09/17 Pct Recovery = 91% Analysis Date = 01/09/17 Pct Recovery = 91% Analysis Date = 01/04/17 Pct Recovery = 91% Analysis Date = 01/04/17 Pct Recovery = 91% Analysis Date = 12/30/16 Pct Recovery = 91% Analysis Date = 12/30/16 Pct Recovery = 91% Analysis Date = 12/25/16 Pct Recovery = 91% Analysis Date = 12/25/16 Pct Recovery = 91% Analysis Date = 12/20/16 Pct Recovery = 91% Analysis Date = 12/20/16 Pct Recovery = 91% Analysis Date = 12/15/16 Pct Recovery = 90% Analysis Date = 12/15/16 Pct Recovery = 90% Analysis Date = 12/10/16 Pct Recovery = 90% Analysis Date = 12/10/16 Pct Recovery = 90% Analysis Date = 12/05/16 Pct Recovery = 90% Analysis Date = 12/05/16 Pct Recovery = 90% Analysis Date = 12/01/16 Pct Recovery = 90% Analysis Date = 12/01/16 Pct Recovery = 90% Analysis Date = 11/26/16 Pct Recovery = 90% Analysis Date = 11/26/16 Pct Recovery = 90% Analysis Date = 11/21/16 Pct Recovery = 90% Analysis Date = 11/21/16 Pct Recovery = 90% Analysis Date = 11/16/16 Pct Recovery = 90% Analysis Date = 11/16/16 Pct Recovery = 90% Analysis Date = 11/11/16 Pct Recovery = 89% Analysis Date = 11/11/16 Pct Recovery = 89% Analysis Date = 11/06/16 Pct Recovery = 89% Analysis Date = 11/06/16 Pct Recovery = 89% Analysis Date = 11/01/16 Pct Recovery = 89% Analysis Date = 11/01/16 Pct Recovery = 89% Analysis Date = 10/27/16 Pct Recovery = 89% Analysis Date = 10/27/16 Pct Recovery = 89% Analysis Date = 10/22/16 Pct Recovery = 89% Analysis Date = 10/22/16 Pct Recovery = 89% Analysis Date = 10/18/16 Pct Recovery = 89% Analysis Date = 10/18/16 Pct Recovery = 89% Analysis Date = 10/13/16 Pct Recovery = 89% Analysis Date = 10/13/16 Pct Recovery = 89% Analysis Date = 10/08/16 Pct Recovery = 89% Analysis Date = 10/08/16 Pct Recovery = 89% Analysis Date = 10/03/16 Pct Recovery = 88% Analysis Date = 10/03/16 Pct Recovery = 88% Analysis Date = 09/28/16 Pct Recovery = 88% Analysis Date = 09/28/16 Pct Recovery = 88% Analysis Date = 09/23/16 Pct Recovery = 88% Analysis Date = 09/23/16 Pct Recovery = 88% Analysis Date = 09/18/16 Pct Recovery = 88% Analysis Date = 09/18/16 Pct Recovery = 88% Analysis Date = 09/13/16 Pct Recovery = 88% Analysis Date = 09/13/16 Pct Recovery = 88% Analysis Date = 09/08/16 Pct Recovery = 88% Analysis Date = 09/08/16 Pct Recovery = 88% Analysis Date = 09/04/16 Pct Recovery = 88% Analysis Date = 09/04/16 Pct Recovery = 88% Analysis Date = 08/30/16 Pct Recovery = 88% Analysis Date = 08/30/16 Pct Recovery = 88% Analysis Date = 08/25/16 Pct Recovery = 88% Analysis Date = 08/25/16 Pct Recovery = 88% Analysis Date = 08/20/16 Pct Recovery = 88% Analysis Date = 08/20/16 Pct Recovery = 88% Analysis Date = 08/15/16 Pct Recovery = 87% Analysis Date = 08/15/16 Pct Recovery = 87% Analysis Date = 08/10/16 Pct Recovery = 87% Analysis Date = 08/10/16 Pct Recovery = 87% Analysis Date = 08/05/16 Pct Recovery = 87% Analysis Date = 08/05/16 Pct Recovery = 87% Analysis Date = 07/31/16 Pct Recovery = 87% Analysis Date = 07/31/16 Pct Recovery = 87% Analysis Date = 07/26/16 Pct Recovery = 87% Analysis Date = 07/26/16 Pct Recovery = 87% Analysis Date = 07/22/16 Pct Recovery = 87% Analysis Date = 07/22/16 Pct Recovery = 87% Analysis Date = 07/17/16 Pct Recovery = 87% Analysis Date = 07/17/16 Pct Recovery = 87% Analysis Date = 07/12/16 Pct Recovery = 87% Analysis Date = 07/12/16 Pct Recovery = 87% Analysis Date = 07/07/16 Pct Recovery = 87% Analysis Date = 07/07/16 Pct Recovery = 87% Analysis Date = 07/02/16 Pct Recovery = 87% Analysis Date = 07/02/16 Pct Recovery = 87% Analysis Date = 06/27/16 Pct Recovery = 87% Analysis Date = 06/27/16 Pct Recovery = 87% Analysis Date = 06/22/16 Pct Recovery = 87% Analysis Date = 06/22/16 Pct Recovery = 87% Analysis Date = 06/17/16 Pct Recovery = 87% Analysis Date = 06/17/16 Pct Recovery = 87% Analysis Date = 06/12/16 Pct Recovery = 87% Analysis Date = 06/12/16 Pct Recovery = 87% Analysis Date = 06/08/16 Pct Recovery = 87% Analysis Date = 06/08/16 Pct Recovery = 87% Analysis Date = 06/03/16 Pct Recovery = 87% Analysis Date = 06/03/16 Pct Recovery = 87% Analysis Date = 05/29/16 Pct Recovery = 87% Analysis Date = 05/29/16 Pct Recovery = 87% Analysis Date = 05/24/16 Pct Recovery = 87% Analysis Date = 05/24/16 Pct Recovery = 87% Analysis Date = 05/19/16 Pct Recovery = 87% Analysis Date = 05/19/16 Pct Recovery = 87% Analysis Date = 05/14/16 Pct Recovery = 87% Analysis Date = 05/14/16 Pct Recovery = 87% Analysis Date = 05/09/16 Pct Recovery = 87% Analysis Date = 05/09/16 Pct Recovery = 87% Analysis Date = 05/04/16 Pct Recovery = 87% Analysis Date = 05/04/16 Pct Recovery = 87% Analysis Date = 04/29/16 Pct Recovery = 87% Analysis Date = 04/29/16 Pct Recovery = 87% Analysis Date = 04/25/16 Pct Recovery = 87% Analysis Date = 04/25/16 Pct Recovery = 87% Analysis Date = 04/20/16 Pct Recovery = 87% Analysis Date = 04/20/16 Pct Recovery = 87% Analysis Date = 04/15/16 Pct Recovery = 87% Analysis Date = 04/15/16 Pct Recovery = 87% Analysis Date = 04/10/16 Pct Recovery = 87% Analysis Date = 04/10/16 Pct Recovery = 87% Analysis Date = 04/05/16 Pct Recovery = 87% Analysis Date = 04/05/16 Pct Recovery = 87% Analysis Date = 03/31/16 Pct Recovery = 87% Analysis Date = 03/31/16 Pct Recovery = 87% Analysis Date = 03/26/16 Pct Recovery = 87% Analysis Date = 03/26/16 Pct Recovery = 87% Analysis Date = 03/21/16 Pct Recovery = 87% Analysis Date = 03/21/16 Pct Recovery = 87% Analysis Date = 03/16/16 Pct Recovery = 87% Analysis Date = 03/16/16 Pct Recovery = 87% Analysis Date = 03/12/16 Pct Recovery = 87% Analysis Date = 03/12/16 Pct Recovery = 87% Analysis Date = 03/07/16 Pct Recovery = 87% Analysis Date = 03/07/16 Pct Recovery = 87% Analysis Date = 03/02/16 Pct Recovery = 87% Analysis Date = 03/02/16 Pct Recovery = 87% Analysis Date = 02/26/16 Pct Recovery = 87% Analysis Date = 02/26/16 Pct Recovery = 87% Analysis Date = 02/21/16 Pct Recovery = 87% Analysis Date = 02/21/16 Pct Recovery = 87% Analysis Date = 02/16/16 Pct Recovery = 87% Analysis Date = 02/16/16 Pct Recovery = 87% Analysis Date = 02/11/16 Pct Recovery = 86% Analysis Date = 02/11/16 Pct Recovery = 86% Analysis Date = 02/06/16 Pct Recovery = 86% Analysis Date = 02/06/16 Pct Recovery = 86% Analysis Date = 02/01/16 Pct Recovery = 86% Analysis Date = 02/01/16 Pct Recovery = 86% Analysis Date = 01/28/16 Pct Recovery = 86% Analysis Date = 01/28/16 Pct Recovery = 86% Analysis Date = 01/23/16 Pct Recovery = 86% Analysis Date = 01/23/16 Pct Recovery = 86% Analysis Date = 01/18/16 Pct Recovery = 86% Analysis Date = 01/18/16 Pct Recovery = 86% Analysis Date = 01/13/16 Pct Recovery = 86% Analysis Date = 01/13/16 Pct Recovery = 86% Analysis Date = 01/08/16 Pct Recovery = 86% Analysis Date = 01/08/16 Pct Recovery = 86% Analysis Date = 01/03/16 Pct Recovery = 86% Analysis Date = 01/03/16 Pct Recovery = 86% Analysis Date = 12/29/15 Pct Recovery = 86% Analysis Date = 12/29/15 Pct Recovery = 86% Analysis Date = 12/24/15 Pct Recovery = 86% Analysis Date = 12/24/15 Pct Recovery = 86% Analysis Date = 12/19/15 Pct Recovery = 86% Analysis Date = 12/19/15 Pct Recovery = 86% Analysis Date = 12/15/15 Pct Recovery = 86% Analysis Date = 12/15/15 Pct Recovery = 86% Analysis Date = 12/10/15 Pct Recovery = 86% Analysis Date = 12/10/15 Pct Recovery = 86% Analysis Date = 12/05/15 Pct Recovery = 86% Analysis Date = 12/05/15 Pct Recovery = 86% Analysis Date = 11/30/15 Pct Recovery = 86% Analysis Date = 11/30/15 Pct Recovery = 86% Analysis Date = 11/25/15 Pct Recovery = 86% Analysis Date = 11/25/15 Pct Recovery = 86% Analysis Date = 11/20/15 Pct Recovery = 86% Analysis Date = 11/20/15 Pct Recovery = 86% Analysis Date = 11/15/15 Pct Recovery = 86% Analysis Date = 11/15/15 Pct Recovery = 86% Analysis Date = 11/10/15 Pct Recovery = 86% Analysis Date = 11/10/15 Pct Recovery = 86% Analysis Date = 11/05/15 Pct Recovery = 86% Analysis Date = 11/05/15 Pct Recovery = 86% Analysis Date = 11/01/15 Pct Recovery = 86% Analysis Date = 11/01/15 Pct Recovery = 86% Analysis Date = 10/27/15 Pct Recovery = 86% Analysis Date = 10/27/15 Pct Recovery = 86% Analysis Date = 10/22/15 Pct Recovery = 86% Analysis Date = 10/22/15 Pct Recovery = 86% Analysis Date = 10/17/15 Pct Recovery = 86% Analysis Date = 10/17/15 Pct Recovery = 86% Analysis Date = 10/12/15 Pct Recovery = 86% Analysis Date = 10/12/15 Pct Recovery = 86% Analysis Date = 10/07/15 Pct Recovery = 86% Analysis Date = 10/07/15 Pct Recovery = 86% Analysis Date = 10/02/15 Pct Recovery = 86% Analysis Date = 10/02/15 Pct Recovery = 86% Analysis Date = 09/27/15 Pct Recovery = 86% Analysis Date = 09/27/15 Pct Recovery = 86% Analysis Date = 09/22/15 Pct Recovery = 86% Analysis Date = 09/22/15 Pct Recovery = 86% Analysis Date = 09/17/15 Pct Recovery = 86% Analysis Date = 09/17/15 Pct Recovery = 86% Analysis Date = 09/13/15 Pct Recovery = 86% Analysis Date = 09/13/15 Pct Recovery = 86% Analysis Date = 09/08/15 Pct Recovery = 86% Analysis Date = 09/08/15 Pct Recovery = 86% Analysis Date = 09/03/15 Pct Recovery = 86% Analysis Date = 09/03/15 Pct Recovery = 86% Analysis Date = 08/29/15 Pct Recovery = 86% Analysis Date = 08/29/15 Pct Recovery = 86% Analysis Date = 08/24/15 Pct Recovery = 86% Analysis Date = 08/24/15 Pct Recovery = 86% Analysis Date = 08/19/15 Pct Recovery = 86% Analysis Date = 08/19/15 Pct Recovery = 86% Analysis Date = 08/14/15 Pct Recovery = 86% Analysis Date = 08/14/15 Pct Recovery = 86% Analysis Date = 08/09/15 Pct Recovery = 86% Analysis Date = 08/09/15 Pct Recovery = 86% Analysis Date = 08/04/15 Pct Recovery = 86% Analysis Date = 08/04/15 Pct Recovery = 86% Analysis Date = 07/31/15 Pct Recovery = 86% Analysis Date = 07/31/15 Pct Recovery = 86% Analysis Date = 07/26/15 Pct Recovery = 86% Analysis Date = 07/26/15 Pct Recovery = 86% Analysis Date = 07/21/15 Pct Recovery = 86% Analysis Date = 07/21/15 Pct Recovery = 86% Analysis Date = 07/16/15 Pct Recovery = 86% Analysis Date = 07/16/15 Pct Recovery = 86% Analysis Date = 07/11/15 Pct Recovery = 86% Analysis Date = 07/11/15 Pct Recovery = 86% Analysis Date = 07/06/15 Pct Recovery = 86% Analysis Date = 07/06/15 Pct Recovery = 86% Analysis Date = 07/01/15 Pct Recovery = 86% Analysis Date = 07/01/15 Pct Recovery = 86% Analysis Date = 06/26/15 Pct Recovery = 86% Analysis Date = 06/26/15 Pct Recovery = 86% Analysis Date = 06/21/15 Pct Recovery = 86% Analysis Date = 06/21/15 Pct Recovery = 86% Analysis Date = 06/17/15 Pct Recovery = 86% Analysis Date = 06/17/15 Pct Recovery = 86% Analysis Date = 06/12/15 Pct Recovery = 86% Analysis Date = 06/12/15 Pct Recovery = 86% Analysis Date = 06/07/15 Pct Recovery = 86% Analysis Date = 06/07/15 Pct Recovery = 86% Analysis Date = 06/02/15 Pct Recovery = 85% Analysis Date = 06/02/15 Pct Recovery = 85% Analysis Date = 05/28/15 Pct Recovery = 85% Analysis Date = 05/28/15 Pct Recovery = 85% Analysis Date = 05/23/15 Pct Recovery = 85% Analysis Date = 05/23/15 Pct Recovery = 85% Analysis Date = 05/18/15 Pct Recovery = 85% Analysis Date = 05/18/15 Pct Recovery = 85% Analysis Date = 05/13/15 Pct Recovery = 85% Analysis Date = 05/13/15 Pct Recovery = 85% Analysis Date = 05/08/15 Pct Recovery = 85% Analysis Date = 05/08/15 Pct Recovery = 85% Analysis Date = 05/04/15 Pct Recovery = 85% Analysis Date = 05/04/15 Pct Recovery = 85% Analysis Date = 04/29/15 Pct Recovery = 85% Analysis Date = 04/29/15 Pct Recovery = 85% Analysis Date = 04/24/15 Pct Recovery = 85% Analysis Date = 04/24/15 Pct Recovery = 85% Analysis Date = 04/19/15 Pct Recovery = 85% Analysis Date = 04/19/15 Pct Recovery = 85% Analysis Date = 04/14/15 Pct Recovery = 85% Analysis Date = 04/14/15 Pct Recovery = 85% Analysis Date = 04/09/15 Pct Recovery = 85% Analysis Date = 04/09/15 Pct Recovery = 85% Analysis Date = 04/04/15 Pct Recovery = 85% Analysis Date = 04/04/15 Pct Recovery = 85% Analysis Date = 03/30/15 Pct Recovery = 85% Analysis Date = 03/30/15 Pct Recovery = 85% Analysis Date = 03/25/15 Pct Recovery = 85% Analysis Date = 03/25/15 Pct Recovery = 85% Analysis Date = 03/21/15 Pct Recovery = 85% Analysis Date = 03/21/15 Pct Recovery = 85% Analysis Date = 03/16/15 Pct Recovery = 85% Analysis Date = 03/16/15 Pct Recovery = 85% Analysis Date = 03/11/15 Pct Recovery = 85% Analysis Date = 03/11/15 Pct Recovery = 85% Analysis Date = 03/06/15 Pct Recovery = 85% Analysis Date = 03/06/15 Pct Recovery = 85% Analysis Date = 03/01/15 Pct Recovery = 85% Analysis Date = 03/01/15 Pct Recovery = 85% Analysis Date = 02/24/15 Pct Recovery = 85% Analysis Date = 02/24/15 Pct Recovery = 85% Analysis Date = 02/19/15 Pct Recovery = 85% Analysis Date = 02/19/15 Pct Recovery = 85% Analysis Date = 02/14/15 Pct Recovery = 84% Analysis Date = 02/14/15 Pct Recovery = 84% Analysis Date = 02/09/15 Pct Recovery = 84% Analysis Date = 02/09/15 Pct Recovery = 84% Analysis Date = 02/05/15 Pct Recovery = 84% Analysis Date = 02/05/15 Pct Recovery = 84% Analysis Date = 01/31/15 Pct Recovery = 84% Analysis Date = 01/31/15 Pct Recovery = 84% Analysis Date = 01/26/15 Pct Recovery = 84% Analysis Date = 01/26/15 Pct Recovery = 84% Analysis Date = 01/21/15 Pct Recovery = 84% Analysis Date = 01/21/15 Pct Recovery = 84% Analysis Date = 01/16/15 Pct Recovery = 84% Analysis Date = 01/16/15 Pct Recovery = 84% Analysis Date = 01/11/15 Pct Recovery = 84% Analysis Date = 01/11/15 Pct Recovery = 84% Analysis Date = 01/06/15 Pct Recovery = 84% Analysis Date = 01/06/15 Pct Recovery = 84% Analysis Date = 01/01/15 Pct Recovery = 84% Analysis Date = 01/01/15 Pct Recovery = 84% Analysis Date = 12/27/14 Pct Recovery = 84% Analysis Date = 12/27/14 Pct Recovery = 84% Analysis Date = 12/23/14 Pct Recovery = 84% Analysis Date = 12/23/14 Pct Recovery = 84% Analysis Date = 12/18/14 Pct Recovery = 84% Analysis Date = 12/18/14 Pct Recovery = 84% Analysis Date = 12/13/14 Pct Recovery = 84% Analysis Date = 12/13/14 Pct Recovery = 84% Analysis Date = 12/08/14 Pct Recovery = 84% Analysis Date = 12/08/14 Pct Recovery = 84% Analysis Date = 12/03/14 Pct Recovery = 84% Analysis Date = 12/03/14 Pct Recovery = 84% Analysis Date = 11/28/14 Pct Recovery = 84% Analysis Date = 11/28/14 Pct Recovery = 84% Analysis Date = 11/23/14 Pct Recovery = 84% Analysis Date = 11/23/14 Pct Recovery = 84% Analysis Date = 11/18/14 Pct Recovery = 84% Analysis Date = 11/18/14 Pct Recovery = 84% Analysis Date = 11/13/14 Pct Recovery = 84% Analysis Date = 11/13/14 Pct Recovery = 84% Analysis Date = 11/09/14 Pct Recovery = 84% Analysis Date = 11/09/14 Pct Recovery = 84% Analysis Date = 11/04/14 Pct Recovery = 84% Analysis Date = 11/04/14 Pct Recovery = 84% Analysis Date = 10/30/14 Pct Recovery = 84% Analysis Date = 10/30/14 Pct Recovery = 84% Analysis Date = 10/25/14 Pct Recovery = 84% Analysis Date = 10/25/14 Pct Recovery = 84% Analysis Date = 10/20/14 Pct Recovery = 84% Analysis Date = 10/20/14 Pct Recovery = 84% Analysis Date = 10/15/14 Pct Recovery = 84% Analysis Date = 10/15/14 Pct Recovery = 84% Analysis Date = 10/10/14 Pct Recovery = 84% Analysis Date = 10/10/14 Pct Recovery = 84% Analysis Date = 10/05/14 Pct Recovery = 84% Analysis Date = 10/05/14 Pct Recovery = 84% Analysis Date = 09/30/14 Pct Recovery = 83% Analysis Date = 09/30/14 Pct Recovery = 83% Analysis Date = 09/26/14 Pct Recovery = 83% Analysis Date = 09/26/14 Pct Recovery = 83% Analysis Date = 09/21/14 Pct Recovery = 83% Analysis Date = 09/21/14 Pct Recovery = 83% Analysis Date = 09/16/14 Pct Recovery = 83% Analysis Date = 09/16/14 Pct Recovery = 83% Analysis Date = 09/11/14 Pct Recovery = 83% Analysis Date = 09/11/14 Pct Recovery = 83% Analysis Date = 09/06/14 Pct Recovery = 83% Analysis Date = 09/06/14 Pct Recovery = 83% Analysis Date = 09/01/14 Pct Recovery = 83% Analysis Date = 09/01/14 Pct Recovery = 83% Analysis Date = 08/27/14 Pct Recovery = 83% Analysis Date = 08/27/14 Pct Recovery = 83% Analysis Date = 08/22/14 Pct Recovery = 83% Analysis Date = 08/22/14 Pct Recovery = 83% Analysis Date = 08/17/14 Pct Recovery = 83% Analysis Date = 08/17/14 Pct Recovery = 83% Analysis Date = 08/13/14 Pct Recovery = 83% Analysis Date = 08/13/14 Pct Recovery = 83% Analysis Date = 08/08/14 Pct Recovery = 83% Analysis Date = 08/08/14 Pct Recovery = 83% Analysis Date = 08/03/14 Pct Recovery = 83% Analysis Date = 08/03/14 Pct Recovery = 83% Analysis Date = 07/29/14 Pct Recovery = 83% Analysis Date = 07/29/14 Pct Recovery = 83% Analysis Date = 07/24/14 Pct Recovery = 83% Analysis Date = 07/24/14 Pct Recovery = 83% Analysis Date = 07/19/14 Pct Recovery = 83% Analysis Date = 07/19/14 Pct Recovery = 83% Analysis Date = 07/14/14 Pct Recovery = 83% Analysis Date = 07/14/14 Pct Recovery = 83% Analysis Date = 07/09/14 Pct Recovery = 83% Analysis Date = 07/09/14 Pct Recovery = 83% Analysis Date = 07/04/14 Pct Recovery = 83% Analysis Date = 07/04/14 Pct Recovery = 83% Analysis Date = 06/30/14 Pct Recovery = 83% Analysis Date = 06/30/14 Pct Recovery = 83% Analysis Date = 06/25/14 Pct Recovery = 82% Analysis Date = 06/25/14 Pct Recovery = 82% Analysis Date = 06/20/14 Pct Recovery = 82% Analysis Date = 06/20/14 Pct Recovery = 82% Analysis Date = 06/15/14 Pct Recovery = 82% Analysis Date = 06/15/14 Pct Recovery = 82% Analysis Date = 06/10/14 Pct Recovery = 82% Analysis Date = 06/10/14 Pct Recovery = 82% Analysis Date = 06/05/14 Pct Recovery = 82% Analysis Date = 06/05/14 Pct Recovery = 82% Analysis Date = 05/31/14 Pct Recovery = 82% Analysis Date = 05/31/14 Pct Recovery = 82% Analysis Date = 05/26/14 Pct Recovery = 82% Analysis Date = 05/26/14 Pct Recovery = 82% Analysis Date = 05/21/14 Pct Recovery = 82% Analysis Date = 05/21/14 Pct Recovery = 82% Analysis Date = 05/17/14 Pct Recovery = 82% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
PHENYTOIN

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 77 86% 13% 83% 11%
Total 77 86% 13% 83% 11%

Sample Statistics
PHENYTOIN

Characteristic N % % Basis
Plotted 77 99% Spiked
Estimated Values 19 24% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 78 .  
False Negatives 1 1% 1 out of 78
Not Spiked 37 .  
False Positives 0 0% 0 out of 37

BQS OBSP Determination:
PIPERONYL BUTOXIDE
METHOD: 2440 , TESTIDCODE: 67435LCM56
Open Data Set

Analysis Date = 02/23/16 SpikeMix = Abs 050115: 80 µl & ERA 0406-15-08: 80 µl Pct Recovery = 46% Analysis Date = 11/04/15 SpikeMix = Abs 052215: 80 µl & Abs 050115: 80 µl Pct Recovery = 64% Analysis Date = 01/17/16 SpikeMix = ERA 0406-15-09: 80 µl & ERA 0406-15-07A: 80 µl Pct Recovery = 33% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 80 µl & Abs 051315: 80 µl Pct Recovery = 64% Analysis Date = 09/24/16 SpikeMix = Crescent EN160610015: 80 µl & Abs 061416: 80 µl Pct Recovery = 37% Analysis Date = 09/24/16 SpikeMix = Abs 061416: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 29% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 70% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 80% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 99% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 109% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-04: 15 µl & Abs 041814: 15 µl Pct Recovery = 54% Analysis Date = 12/06/14 SpikeMix = ERA 0318-14-02: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 49% Analysis Date = 10/25/14 SpikeMix = Abs 041614: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 40% Analysis Date = 10/11/14 SpikeMix = ERA 0318-14-02: 60 µl & ERA 0319-14-04: 60 µl Pct Recovery = 35% Analysis Date = 08/28/14 SpikeMix = ERA 0319-14-04: 60 µl & ERA 0319-14-05: 60 µl Pct Recovery = 52% Analysis Date = 05/07/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 71% Analysis Date = 03/11/15 SpikeMix = ERA 0318-14-02: 15 µl & Abs 041714: 15 µl Pct Recovery = 46% Analysis Date = 01/16/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 67% Analysis Date = 12/06/14 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 56% Analysis Date = 08/21/14 SpikeMix = ERA 0318-14-02: 60 µl & Abs 041714: 60 µl Pct Recovery = 44% Analysis Date = 07/12/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 42% Analysis Date = 05/21/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 51% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 87% Analysis Date = 02/23/16 SpikeMix = Abs 052215: 40 µl & Abs 050115: 40 µl Pct Recovery = 89% Analysis Date = 07/31/15 SpikeMix = ERA 0406-15-09: 40 µl & Abs 050115: 40 µl Pct Recovery = 69% Analysis Date = 07/30/15 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 62% Analysis Date = 11/04/15 SpikeMix = ERA 0406-15-07A: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 54% Analysis Date = 09/10/15 SpikeMix = Abs 052215: 40 µl & ERA 0406-15-07A: 40 µl Pct Recovery = 69% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 39% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 38% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 35% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 36% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 26% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 46% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 37% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 41% Analysis Date = 04/30/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 68% Analysis Date = 04/10/15 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 23% Analysis Date = 02/10/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 74% Analysis Date = 12/07/14 SpikeMix = ERA 0318-14-02: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 56% Analysis Date = 10/11/14 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 7% Analysis Date = 11/04/14 SpikeMix = Abs 041714: 8 µl & ERA 0319-14-05: 8 µl Pct Recovery = 9% Analysis Date = 09/12/14 SpikeMix = Abs 041614: 30 µl & ERA 0319-14-04: 30 µl Pct Recovery = 37% Analysis Date = 08/16/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 34% Analysis Date = 10/10/14 SpikeMix = Abs 041714: 30 µl & Abs 041814: 30 µl Pct Recovery = 18% Analysis Date = 07/20/14 SpikeMix = ERA 0318-14-02: 30 µl & Abs 041714: 30 µl Pct Recovery = 34% Analysis Date = 05/17/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 132% Analysis Date = 04/23/14 SpikeMix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.2: 20 µl Pct Recovery = 53% Analysis Date = 11/25/15 SpikeMix = Abs 050115: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 67% Analysis Date = 11/24/15 SpikeMix = ERA 0406-15-09: 20 µl & Abs 050115: 20 µl Pct Recovery = 63% Analysis Date = 08/27/15 SpikeMix = Abs 052215: 20 µl & Abs 050115: 20 µl Pct Recovery = 67% Analysis Date = 08/11/15 SpikeMix = Abs 050115: 20 µl & Abs 051315: 20 µl Pct Recovery = 48% Analysis Date = 07/09/15 SpikeMix = Abs 050115: 20 µl & Abs 052215: 20 µl Pct Recovery = 40% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 88% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 22% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 52% Analysis Date = 11/24/15 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 73% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-09: 20 µl Pct Recovery = 67% Analysis Date = 09/15/15 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 67% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 42% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 35% Analysis Date = 11/18/16 SpikeMix = ERA 04281604: 80 µl & ERA 04281603: 80 µl Pct Recovery = 32% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & ERA 04281604: 80 µl Pct Recovery = 41% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 93% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 71% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 65% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 17% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 24% Analysis Date = 01/04/17 Pct Recovery = 41% Analysis Date = 12/31/16 Pct Recovery = 41% Analysis Date = 12/31/16 Pct Recovery = 41% Analysis Date = 12/26/16 Pct Recovery = 41% Analysis Date = 12/26/16 Pct Recovery = 41% Analysis Date = 12/21/16 Pct Recovery = 42% Analysis Date = 12/21/16 Pct Recovery = 42% Analysis Date = 12/16/16 Pct Recovery = 42% Analysis Date = 12/16/16 Pct Recovery = 42% Analysis Date = 12/11/16 Pct Recovery = 43% Analysis Date = 12/11/16 Pct Recovery = 43% Analysis Date = 12/06/16 Pct Recovery = 43% Analysis Date = 12/06/16 Pct Recovery = 43% Analysis Date = 12/01/16 Pct Recovery = 43% Analysis Date = 12/01/16 Pct Recovery = 43% Analysis Date = 11/26/16 Pct Recovery = 44% Analysis Date = 11/26/16 Pct Recovery = 44% Analysis Date = 11/21/16 Pct Recovery = 44% Analysis Date = 11/21/16 Pct Recovery = 44% Analysis Date = 11/16/16 Pct Recovery = 45% Analysis Date = 11/16/16 Pct Recovery = 45% Analysis Date = 11/11/16 Pct Recovery = 45% Analysis Date = 11/11/16 Pct Recovery = 45% Analysis Date = 11/06/16 Pct Recovery = 45% Analysis Date = 11/06/16 Pct Recovery = 45% Analysis Date = 11/01/16 Pct Recovery = 46% Analysis Date = 11/01/16 Pct Recovery = 46% Analysis Date = 10/27/16 Pct Recovery = 46% Analysis Date = 10/27/16 Pct Recovery = 46% Analysis Date = 10/22/16 Pct Recovery = 47% Analysis Date = 10/22/16 Pct Recovery = 47% Analysis Date = 10/17/16 Pct Recovery = 47% Analysis Date = 10/17/16 Pct Recovery = 47% Analysis Date = 10/13/16 Pct Recovery = 47% Analysis Date = 10/13/16 Pct Recovery = 47% Analysis Date = 10/08/16 Pct Recovery = 48% Analysis Date = 10/08/16 Pct Recovery = 48% Analysis Date = 10/03/16 Pct Recovery = 48% Analysis Date = 10/03/16 Pct Recovery = 48% Analysis Date = 09/28/16 Pct Recovery = 48% Analysis Date = 09/28/16 Pct Recovery = 48% Analysis Date = 09/23/16 Pct Recovery = 49% Analysis Date = 09/23/16 Pct Recovery = 49% Analysis Date = 09/18/16 Pct Recovery = 49% Analysis Date = 09/18/16 Pct Recovery = 49% Analysis Date = 09/13/16 Pct Recovery = 50% Analysis Date = 09/13/16 Pct Recovery = 50% Analysis Date = 09/08/16 Pct Recovery = 50% Analysis Date = 09/08/16 Pct Recovery = 50% Analysis Date = 09/03/16 Pct Recovery = 50% Analysis Date = 09/03/16 Pct Recovery = 50% Analysis Date = 08/29/16 Pct Recovery = 51% Analysis Date = 08/29/16 Pct Recovery = 51% Analysis Date = 08/24/16 Pct Recovery = 51% Analysis Date = 08/24/16 Pct Recovery = 51% Analysis Date = 08/19/16 Pct Recovery = 51% Analysis Date = 08/19/16 Pct Recovery = 51% Analysis Date = 08/14/16 Pct Recovery = 52% Analysis Date = 08/14/16 Pct Recovery = 52% Analysis Date = 08/09/16 Pct Recovery = 52% Analysis Date = 08/09/16 Pct Recovery = 52% Analysis Date = 08/04/16 Pct Recovery = 52% Analysis Date = 08/04/16 Pct Recovery = 52% Analysis Date = 07/30/16 Pct Recovery = 53% Analysis Date = 07/30/16 Pct Recovery = 53% Analysis Date = 07/25/16 Pct Recovery = 53% Analysis Date = 07/25/16 Pct Recovery = 53% Analysis Date = 07/21/16 Pct Recovery = 53% Analysis Date = 07/21/16 Pct Recovery = 53% Analysis Date = 07/16/16 Pct Recovery = 53% Analysis Date = 07/16/16 Pct Recovery = 53% Analysis Date = 07/11/16 Pct Recovery = 54% Analysis Date = 07/11/16 Pct Recovery = 54% Analysis Date = 07/06/16 Pct Recovery = 54% Analysis Date = 07/06/16 Pct Recovery = 54% Analysis Date = 07/01/16 Pct Recovery = 54% Analysis Date = 07/01/16 Pct Recovery = 54% Analysis Date = 06/26/16 Pct Recovery = 55% Analysis Date = 06/26/16 Pct Recovery = 55% Analysis Date = 06/21/16 Pct Recovery = 55% Analysis Date = 06/21/16 Pct Recovery = 55% Analysis Date = 06/16/16 Pct Recovery = 55% Analysis Date = 06/16/16 Pct Recovery = 55% Analysis Date = 06/11/16 Pct Recovery = 56% Analysis Date = 06/11/16 Pct Recovery = 56% Analysis Date = 06/06/16 Pct Recovery = 56% Analysis Date = 06/06/16 Pct Recovery = 56% Analysis Date = 06/01/16 Pct Recovery = 56% Analysis Date = 06/01/16 Pct Recovery = 56% Analysis Date = 05/27/16 Pct Recovery = 57% Analysis Date = 05/27/16 Pct Recovery = 57% Analysis Date = 05/22/16 Pct Recovery = 57% Analysis Date = 05/22/16 Pct Recovery = 57% Analysis Date = 05/17/16 Pct Recovery = 57% Analysis Date = 05/17/16 Pct Recovery = 57% Analysis Date = 05/12/16 Pct Recovery = 58% Analysis Date = 05/12/16 Pct Recovery = 58% Analysis Date = 05/07/16 Pct Recovery = 58% Analysis Date = 05/07/16 Pct Recovery = 58% Analysis Date = 05/02/16 Pct Recovery = 58% Analysis Date = 05/02/16 Pct Recovery = 58% Analysis Date = 04/28/16 Pct Recovery = 58% Analysis Date = 04/28/16 Pct Recovery = 58% Analysis Date = 04/23/16 Pct Recovery = 59% Analysis Date = 04/23/16 Pct Recovery = 59% Analysis Date = 04/18/16 Pct Recovery = 59% Analysis Date = 04/18/16 Pct Recovery = 59% Analysis Date = 04/13/16 Pct Recovery = 59% Analysis Date = 04/13/16 Pct Recovery = 59% Analysis Date = 04/08/16 Pct Recovery = 60% Analysis Date = 04/08/16 Pct Recovery = 60% Analysis Date = 04/03/16 Pct Recovery = 60% Analysis Date = 04/03/16 Pct Recovery = 60% Analysis Date = 03/29/16 Pct Recovery = 60% Analysis Date = 03/29/16 Pct Recovery = 60% Analysis Date = 03/24/16 Pct Recovery = 61% Analysis Date = 03/24/16 Pct Recovery = 61% Analysis Date = 03/19/16 Pct Recovery = 61% Analysis Date = 03/19/16 Pct Recovery = 61% Analysis Date = 03/14/16 Pct Recovery = 61% Analysis Date = 03/14/16 Pct Recovery = 61% Analysis Date = 03/09/16 Pct Recovery = 62% Analysis Date = 03/09/16 Pct Recovery = 62% Analysis Date = 03/04/16 Pct Recovery = 62% Analysis Date = 03/04/16 Pct Recovery = 62% Analysis Date = 02/28/16 Pct Recovery = 62% Analysis Date = 02/28/16 Pct Recovery = 62% Analysis Date = 02/23/16 Pct Recovery = 62% Analysis Date = 02/23/16 Pct Recovery = 62% Analysis Date = 02/18/16 Pct Recovery = 62% Analysis Date = 02/18/16 Pct Recovery = 62% Analysis Date = 02/13/16 Pct Recovery = 62% Analysis Date = 02/13/16 Pct Recovery = 62% Analysis Date = 02/09/16 Pct Recovery = 62% Analysis Date = 02/09/16 Pct Recovery = 62% Analysis Date = 02/04/16 Pct Recovery = 62% Analysis Date = 02/04/16 Pct Recovery = 62% Analysis Date = 01/30/16 Pct Recovery = 62% Analysis Date = 01/30/16 Pct Recovery = 62% Analysis Date = 01/25/16 Pct Recovery = 63% Analysis Date = 01/25/16 Pct Recovery = 63% Analysis Date = 01/20/16 Pct Recovery = 63% Analysis Date = 01/20/16 Pct Recovery = 63% Analysis Date = 01/15/16 Pct Recovery = 63% Analysis Date = 01/15/16 Pct Recovery = 63% Analysis Date = 01/10/16 Pct Recovery = 63% Analysis Date = 01/10/16 Pct Recovery = 63% Analysis Date = 01/05/16 Pct Recovery = 63% Analysis Date = 01/05/16 Pct Recovery = 63% Analysis Date = 12/31/15 Pct Recovery = 62% Analysis Date = 12/31/15 Pct Recovery = 62% Analysis Date = 12/26/15 Pct Recovery = 62% Analysis Date = 12/26/15 Pct Recovery = 62% Analysis Date = 12/21/15 Pct Recovery = 62% Analysis Date = 12/21/15 Pct Recovery = 62% Analysis Date = 12/16/15 Pct Recovery = 62% Analysis Date = 12/16/15 Pct Recovery = 62% Analysis Date = 12/11/15 Pct Recovery = 62% Analysis Date = 12/11/15 Pct Recovery = 62% Analysis Date = 12/06/15 Pct Recovery = 62% Analysis Date = 12/06/15 Pct Recovery = 62% Analysis Date = 12/01/15 Pct Recovery = 62% Analysis Date = 12/01/15 Pct Recovery = 62% Analysis Date = 11/26/15 Pct Recovery = 62% Analysis Date = 11/26/15 Pct Recovery = 62% Analysis Date = 11/21/15 Pct Recovery = 62% Analysis Date = 11/21/15 Pct Recovery = 62% Analysis Date = 11/17/15 Pct Recovery = 62% Analysis Date = 11/17/15 Pct Recovery = 62% Analysis Date = 11/12/15 Pct Recovery = 62% Analysis Date = 11/12/15 Pct Recovery = 62% Analysis Date = 11/07/15 Pct Recovery = 62% Analysis Date = 11/07/15 Pct Recovery = 62% Analysis Date = 11/02/15 Pct Recovery = 62% Analysis Date = 11/02/15 Pct Recovery = 62% Analysis Date = 10/28/15 Pct Recovery = 62% Analysis Date = 10/28/15 Pct Recovery = 62% Analysis Date = 10/23/15 Pct Recovery = 61% Analysis Date = 10/23/15 Pct Recovery = 61% Analysis Date = 10/18/15 Pct Recovery = 61% Analysis Date = 10/18/15 Pct Recovery = 61% Analysis Date = 10/13/15 Pct Recovery = 61% Analysis Date = 10/13/15 Pct Recovery = 61% Analysis Date = 10/08/15 Pct Recovery = 61% Analysis Date = 10/08/15 Pct Recovery = 61% Analysis Date = 10/03/15 Pct Recovery = 61% Analysis Date = 10/03/15 Pct Recovery = 61% Analysis Date = 09/28/15 Pct Recovery = 61% Analysis Date = 09/28/15 Pct Recovery = 61% Analysis Date = 09/23/15 Pct Recovery = 61% Analysis Date = 09/23/15 Pct Recovery = 61% Analysis Date = 09/18/15 Pct Recovery = 60% Analysis Date = 09/18/15 Pct Recovery = 60% Analysis Date = 09/13/15 Pct Recovery = 60% Analysis Date = 09/13/15 Pct Recovery = 60% Analysis Date = 09/08/15 Pct Recovery = 60% Analysis Date = 09/08/15 Pct Recovery = 60% Analysis Date = 09/03/15 Pct Recovery = 60% Analysis Date = 09/03/15 Pct Recovery = 60% Analysis Date = 08/29/15 Pct Recovery = 60% Analysis Date = 08/29/15 Pct Recovery = 60% Analysis Date = 08/25/15 Pct Recovery = 60% Analysis Date = 08/25/15 Pct Recovery = 60% Analysis Date = 08/20/15 Pct Recovery = 60% Analysis Date = 08/20/15 Pct Recovery = 60% Analysis Date = 08/15/15 Pct Recovery = 59% Analysis Date = 08/15/15 Pct Recovery = 59% Analysis Date = 08/10/15 Pct Recovery = 59% Analysis Date = 08/10/15 Pct Recovery = 59% Analysis Date = 08/05/15 Pct Recovery = 59% Analysis Date = 08/05/15 Pct Recovery = 59% Analysis Date = 07/31/15 Pct Recovery = 59% Analysis Date = 07/31/15 Pct Recovery = 59% Analysis Date = 07/26/15 Pct Recovery = 59% Analysis Date = 07/26/15 Pct Recovery = 59% Analysis Date = 07/21/15 Pct Recovery = 58% Analysis Date = 07/21/15 Pct Recovery = 58% Analysis Date = 07/16/15 Pct Recovery = 58% Analysis Date = 07/16/15 Pct Recovery = 58% Analysis Date = 07/11/15 Pct Recovery = 58% Analysis Date = 07/11/15 Pct Recovery = 58% Analysis Date = 07/06/15 Pct Recovery = 58% Analysis Date = 07/06/15 Pct Recovery = 58% Analysis Date = 07/01/15 Pct Recovery = 57% Analysis Date = 07/01/15 Pct Recovery = 57% Analysis Date = 06/26/15 Pct Recovery = 57% Analysis Date = 06/26/15 Pct Recovery = 57% Analysis Date = 06/21/15 Pct Recovery = 57% Analysis Date = 06/21/15 Pct Recovery = 57% Analysis Date = 06/16/15 Pct Recovery = 57% Analysis Date = 06/16/15 Pct Recovery = 57% Analysis Date = 06/11/15 Pct Recovery = 56% Analysis Date = 06/11/15 Pct Recovery = 56% Analysis Date = 06/07/15 Pct Recovery = 56% Analysis Date = 06/07/15 Pct Recovery = 56% Analysis Date = 06/02/15 Pct Recovery = 56% Analysis Date = 06/02/15 Pct Recovery = 56% Analysis Date = 05/28/15 Pct Recovery = 55% Analysis Date = 05/28/15 Pct Recovery = 55% Analysis Date = 05/23/15 Pct Recovery = 55% Analysis Date = 05/23/15 Pct Recovery = 55% Analysis Date = 05/18/15 Pct Recovery = 55% Analysis Date = 05/18/15 Pct Recovery = 55% Analysis Date = 05/13/15 Pct Recovery = 55% Analysis Date = 05/13/15 Pct Recovery = 55% Analysis Date = 05/08/15 Pct Recovery = 54% Analysis Date = 05/08/15 Pct Recovery = 54% Analysis Date = 05/03/15 Pct Recovery = 54% Analysis Date = 05/03/15 Pct Recovery = 54% Analysis Date = 04/28/15 Pct Recovery = 54% Analysis Date = 04/28/15 Pct Recovery = 54% Analysis Date = 04/23/15 Pct Recovery = 53% Analysis Date = 04/23/15 Pct Recovery = 53% Analysis Date = 04/18/15 Pct Recovery = 53% Analysis Date = 04/18/15 Pct Recovery = 53% Analysis Date = 04/13/15 Pct Recovery = 53% Analysis Date = 04/13/15 Pct Recovery = 53% Analysis Date = 04/08/15 Pct Recovery = 53% Analysis Date = 04/08/15 Pct Recovery = 53% Analysis Date = 04/03/15 Pct Recovery = 52% Analysis Date = 04/03/15 Pct Recovery = 52% Analysis Date = 03/29/15 Pct Recovery = 52% Analysis Date = 03/29/15 Pct Recovery = 52% Analysis Date = 03/24/15 Pct Recovery = 52% Analysis Date = 03/24/15 Pct Recovery = 52% Analysis Date = 03/19/15 Pct Recovery = 52% Analysis Date = 03/19/15 Pct Recovery = 52% Analysis Date = 03/15/15 Pct Recovery = 52% Analysis Date = 03/15/15 Pct Recovery = 52% Analysis Date = 03/10/15 Pct Recovery = 52% Analysis Date = 03/10/15 Pct Recovery = 52% Analysis Date = 03/05/15 Pct Recovery = 51% Analysis Date = 03/05/15 Pct Recovery = 51% Analysis Date = 02/28/15 Pct Recovery = 51% Analysis Date = 02/28/15 Pct Recovery = 51% Analysis Date = 02/23/15 Pct Recovery = 51% Analysis Date = 02/23/15 Pct Recovery = 51% Analysis Date = 02/18/15 Pct Recovery = 51% Analysis Date = 02/18/15 Pct Recovery = 51% Analysis Date = 02/13/15 Pct Recovery = 51% Analysis Date = 02/13/15 Pct Recovery = 51% Analysis Date = 02/08/15 Pct Recovery = 51% Analysis Date = 02/08/15 Pct Recovery = 51% Analysis Date = 02/03/15 Pct Recovery = 51% Analysis Date = 02/03/15 Pct Recovery = 51% Analysis Date = 01/29/15 Pct Recovery = 50% Analysis Date = 01/29/15 Pct Recovery = 50% Analysis Date = 01/24/15 Pct Recovery = 50% Analysis Date = 01/24/15 Pct Recovery = 50% Analysis Date = 01/19/15 Pct Recovery = 50% Analysis Date = 01/19/15 Pct Recovery = 50% Analysis Date = 01/14/15 Pct Recovery = 50% Analysis Date = 01/14/15 Pct Recovery = 50% Analysis Date = 01/09/15 Pct Recovery = 50% Analysis Date = 01/09/15 Pct Recovery = 50% Analysis Date = 01/04/15 Pct Recovery = 50% Analysis Date = 01/04/15 Pct Recovery = 50% Analysis Date = 12/30/14 Pct Recovery = 49% Analysis Date = 12/30/14 Pct Recovery = 49% Analysis Date = 12/25/14 Pct Recovery = 49% Analysis Date = 12/25/14 Pct Recovery = 49% Analysis Date = 12/21/14 Pct Recovery = 49% Analysis Date = 12/21/14 Pct Recovery = 49% Analysis Date = 12/16/14 Pct Recovery = 49% Analysis Date = 12/16/14 Pct Recovery = 49% Analysis Date = 12/11/14 Pct Recovery = 49% Analysis Date = 12/11/14 Pct Recovery = 49% Analysis Date = 12/06/14 Pct Recovery = 49% Analysis Date = 12/06/14 Pct Recovery = 49% Analysis Date = 12/01/14 Pct Recovery = 49% Analysis Date = 12/01/14 Pct Recovery = 49% Analysis Date = 11/26/14 Pct Recovery = 49% Analysis Date = 11/26/14 Pct Recovery = 49% Analysis Date = 11/21/14 Pct Recovery = 48% Analysis Date = 11/21/14 Pct Recovery = 48% Analysis Date = 11/16/14 Pct Recovery = 48% Analysis Date = 11/16/14 Pct Recovery = 48% Analysis Date = 11/11/14 Pct Recovery = 48% Analysis Date = 11/11/14 Pct Recovery = 48% Analysis Date = 11/06/14 Pct Recovery = 48% Analysis Date = 11/06/14 Pct Recovery = 48% Analysis Date = 11/01/14 Pct Recovery = 48% Analysis Date = 11/01/14 Pct Recovery = 48% Analysis Date = 10/27/14 Pct Recovery = 48% Analysis Date = 10/27/14 Pct Recovery = 48% Analysis Date = 10/22/14 Pct Recovery = 48% Analysis Date = 10/22/14 Pct Recovery = 48% Analysis Date = 10/17/14 Pct Recovery = 48% Analysis Date = 10/17/14 Pct Recovery = 48% Analysis Date = 10/12/14 Pct Recovery = 48% Analysis Date = 10/12/14 Pct Recovery = 48% Analysis Date = 10/07/14 Pct Recovery = 48% Analysis Date = 10/07/14 Pct Recovery = 48% Analysis Date = 10/03/14 Pct Recovery = 48% Analysis Date = 10/03/14 Pct Recovery = 48% Analysis Date = 09/28/14 Pct Recovery = 48% Analysis Date = 09/28/14 Pct Recovery = 48% Analysis Date = 09/23/14 Pct Recovery = 48% Analysis Date = 09/23/14 Pct Recovery = 48% Analysis Date = 09/18/14 Pct Recovery = 48% Analysis Date = 09/18/14 Pct Recovery = 48% Analysis Date = 09/13/14 Pct Recovery = 48% Analysis Date = 09/13/14 Pct Recovery = 48% Analysis Date = 09/08/14 Pct Recovery = 48% Analysis Date = 09/08/14 Pct Recovery = 48% Analysis Date = 09/03/14 Pct Recovery = 48% Analysis Date = 09/03/14 Pct Recovery = 48% Analysis Date = 08/29/14 Pct Recovery = 47% Analysis Date = 08/29/14 Pct Recovery = 47% Analysis Date = 08/24/14 Pct Recovery = 47% Analysis Date = 08/24/14 Pct Recovery = 47% Analysis Date = 08/19/14 Pct Recovery = 47% Analysis Date = 08/19/14 Pct Recovery = 47% Analysis Date = 08/14/14 Pct Recovery = 47% Analysis Date = 08/14/14 Pct Recovery = 47% Analysis Date = 08/09/14 Pct Recovery = 47% Analysis Date = 08/09/14 Pct Recovery = 47% Analysis Date = 08/04/14 Pct Recovery = 47% Analysis Date = 08/04/14 Pct Recovery = 47% Analysis Date = 07/30/14 Pct Recovery = 47% Analysis Date = 07/30/14 Pct Recovery = 47% Analysis Date = 07/25/14 Pct Recovery = 47% Analysis Date = 07/25/14 Pct Recovery = 47% Analysis Date = 07/20/14 Pct Recovery = 47% Analysis Date = 07/20/14 Pct Recovery = 47% Analysis Date = 07/15/14 Pct Recovery = 47% Analysis Date = 07/15/14 Pct Recovery = 47% Analysis Date = 07/11/14 Pct Recovery = 47% Analysis Date = 07/11/14 Pct Recovery = 47% Analysis Date = 07/06/14 Pct Recovery = 47% Analysis Date = 07/06/14 Pct Recovery = 47% Analysis Date = 07/01/14 Pct Recovery = 47% Analysis Date = 07/01/14 Pct Recovery = 47% Analysis Date = 06/26/14 Pct Recovery = 47% Analysis Date = 06/26/14 Pct Recovery = 47% Analysis Date = 06/21/14 Pct Recovery = 47% Analysis Date = 06/21/14 Pct Recovery = 47% Analysis Date = 06/16/14 Pct Recovery = 47% Analysis Date = 06/16/14 Pct Recovery = 47% Analysis Date = 06/11/14 Pct Recovery = 47% Analysis Date = 06/11/14 Pct Recovery = 47% Analysis Date = 06/06/14 Pct Recovery = 47% Analysis Date = 06/06/14 Pct Recovery = 47% Analysis Date = 06/01/14 Pct Recovery = 47% Analysis Date = 06/01/14 Pct Recovery = 47% Analysis Date = 05/27/14 Pct Recovery = 47% Analysis Date = 05/27/14 Pct Recovery = 47% Analysis Date = 05/22/14 Pct Recovery = 47% Analysis Date = 05/22/14 Pct Recovery = 47% Analysis Date = 05/17/14 Pct Recovery = 47% Analysis Date = 05/17/14 Pct Recovery = 47% Analysis Date = 05/12/14 Pct Recovery = 47% Analysis Date = 05/12/14 Pct Recovery = 47% Analysis Date = 05/07/14 Pct Recovery = 47% Analysis Date = 05/07/14 Pct Recovery = 47% Analysis Date = 05/02/14 Pct Recovery = 47% Analysis Date = 05/02/14 Pct Recovery = 47% Analysis Date = 04/27/14 Pct Recovery = 47% Analysis Date = 04/27/14 Pct Recovery = 47% Analysis Date = 04/23/14 Pct Recovery = 47% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
PIPERONYL BUTOXIDE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 9 47% 25% 41% 25%
>= Reporting Level 59 54% 23% 52% 22%
Total 68 53% 24% 50% 23%

Sample Statistics
PIPERONYL BUTOXIDE

Characteristic N % % Basis
Plotted 68 86% Spiked
Estimated Values 35 44% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 5 6% Spiked
Spiked 79 .  
False Negatives 6 8% 6 out of 79
Not Spiked 36 .  
False Positives 0 0% 0 out of 36

BQS OBSP Determination:
PREDNISOLONE
METHOD: 2440 , TESTIDCODE: 67483LCM56
Open Data Set

Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 91% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 91% Analysis Date = 01/17/16 SpikeMix = ERA 0406-15-09: 80 µl & ERA 0406-15-07A: 80 µl Pct Recovery = 71% Analysis Date = 11/24/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 79% Analysis Date = 11/05/15 SpikeMix = ERA 0406-15-08: 80 µl & Abs 052215: 80 µl Pct Recovery = 76% Analysis Date = 11/04/15 SpikeMix = Abs 052215: 80 µl & Abs 050115: 80 µl Pct Recovery = 79% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 74% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 78% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 93% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 91% Analysis Date = 11/18/16 SpikeMix = ERA 04281604: 80 µl & ERA 04281603: 80 µl Pct Recovery = 74% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & ERA 04281604: 80 µl Pct Recovery = 73% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 67% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 68% Analysis Date = 05/07/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 98% Analysis Date = 03/11/15 SpikeMix = ERA 0318-14-02: 15 µl & Abs 041714: 15 µl Pct Recovery = 96% Analysis Date = 01/16/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 93% Analysis Date = 12/06/14 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 66% Analysis Date = 08/21/14 SpikeMix = ERA 0318-14-02: 60 µl & Abs 041714: 60 µl Pct Recovery = 72% Analysis Date = 07/12/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 77% Analysis Date = 06/11/14 SpikeMix = Abs 041614: 60 µl & Abs 041714: 60 µl Pct Recovery = 89% Analysis Date = 05/21/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 81% Analysis Date = 12/06/14 SpikeMix = ERA 0318-14-02: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 70% Analysis Date = 10/25/14 SpikeMix = Abs 041614: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 74% Analysis Date = 10/11/14 SpikeMix = ERA 0318-14-02: 60 µl & ERA 0319-14-04: 60 µl Pct Recovery = 68% Analysis Date = 08/28/14 SpikeMix = ERA 0319-14-04: 60 µl & ERA 0319-14-05: 60 µl Pct Recovery = 71% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-08: 40 µl & ERA 0406-15-09: 40 µl Pct Recovery = 74% Analysis Date = 07/31/15 SpikeMix = ERA 0406-15-09: 40 µl & Abs 050115: 40 µl Pct Recovery = 85% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-08: 40 µl & Abs 052215: 40 µl Pct Recovery = 101% Analysis Date = 02/23/16 SpikeMix = Abs 052215: 40 µl & Abs 050115: 40 µl Pct Recovery = 84% Analysis Date = 09/10/15 SpikeMix = Abs 052215: 40 µl & ERA 0406-15-07A: 40 µl Pct Recovery = 87% Analysis Date = 07/31/15 SpikeMix = Abs 051315: 40 µl & Abs 052215: 40 µl Pct Recovery = 76% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 122% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 117% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 86% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 83% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 79% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 82% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 65% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 67% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 60% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 75% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 65% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 71% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 65% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 69% Analysis Date = 11/04/14 SpikeMix = Abs 041714: 8 µl & ERA 0319-14-05: 8 µl Pct Recovery = 71% Analysis Date = 04/30/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 74% Analysis Date = 04/10/15 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 90% Analysis Date = 02/10/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 71% Analysis Date = 12/07/14 SpikeMix = ERA 0318-14-02: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 67% Analysis Date = 10/11/14 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 77% Analysis Date = 10/10/14 SpikeMix = Abs 041714: 30 µl & Abs 041814: 30 µl Pct Recovery = 69% Analysis Date = 07/20/14 SpikeMix = ERA 0318-14-02: 30 µl & Abs 041714: 30 µl Pct Recovery = 71% Analysis Date = 06/28/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 79% Analysis Date = 05/17/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 85% Analysis Date = 09/12/14 SpikeMix = Abs 041614: 30 µl & ERA 0319-14-04: 30 µl Pct Recovery = 74% Analysis Date = 08/16/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 57% Analysis Date = 07/13/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 80% Analysis Date = 04/23/14 SpikeMix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.2: 20 µl Pct Recovery = 69% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 96% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 96% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-08: 20 µl & ERA 0406-15-09: 20 µl Pct Recovery = 83% Analysis Date = 11/24/15 SpikeMix = ERA 0406-15-09: 20 µl & Abs 050115: 20 µl Pct Recovery = 79% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 58% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 66% Analysis Date = 02/23/16 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 36% Analysis Date = 11/24/15 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 80% Analysis Date = 09/09/15 SpikeMix = ERA 0406-15-08: 20 µl & Abs 052215: 20 µl Pct Recovery = 103% Analysis Date = 08/27/15 SpikeMix = Abs 052215: 20 µl & Abs 050115: 20 µl Pct Recovery = 81% Analysis Date = 07/09/15 SpikeMix = Abs 050115: 20 µl & Abs 052215: 20 µl Pct Recovery = 73% Analysis Date = 06/26/15 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 70% Analysis Date = 04/09/16 SpikeMix = Abs 051315: 10 µl & ERA 0406-15-09: 10 µl Pct Recovery = 80% Analysis Date = 04/09/16 SpikeMix = Abs 051315: 10 µl & ERA 0406-15-09: 10 µl Pct Recovery = 116% Analysis Date = 01/18/17 Pct Recovery = 84% Analysis Date = 01/13/17 Pct Recovery = 84% Analysis Date = 01/13/17 Pct Recovery = 84% Analysis Date = 01/08/17 Pct Recovery = 83% Analysis Date = 01/08/17 Pct Recovery = 83% Analysis Date = 01/03/17 Pct Recovery = 83% Analysis Date = 01/03/17 Pct Recovery = 83% Analysis Date = 12/29/16 Pct Recovery = 83% Analysis Date = 12/29/16 Pct Recovery = 83% Analysis Date = 12/24/16 Pct Recovery = 83% Analysis Date = 12/24/16 Pct Recovery = 83% Analysis Date = 12/19/16 Pct Recovery = 83% Analysis Date = 12/19/16 Pct Recovery = 83% Analysis Date = 12/14/16 Pct Recovery = 83% Analysis Date = 12/14/16 Pct Recovery = 83% Analysis Date = 12/09/16 Pct Recovery = 82% Analysis Date = 12/09/16 Pct Recovery = 82% Analysis Date = 12/04/16 Pct Recovery = 82% Analysis Date = 12/04/16 Pct Recovery = 82% Analysis Date = 11/29/16 Pct Recovery = 82% Analysis Date = 11/29/16 Pct Recovery = 82% Analysis Date = 11/24/16 Pct Recovery = 82% Analysis Date = 11/24/16 Pct Recovery = 82% Analysis Date = 11/19/16 Pct Recovery = 82% Analysis Date = 11/19/16 Pct Recovery = 82% Analysis Date = 11/14/16 Pct Recovery = 82% Analysis Date = 11/14/16 Pct Recovery = 82% Analysis Date = 11/09/16 Pct Recovery = 81% Analysis Date = 11/09/16 Pct Recovery = 81% Analysis Date = 11/04/16 Pct Recovery = 81% Analysis Date = 11/04/16 Pct Recovery = 81% Analysis Date = 10/30/16 Pct Recovery = 81% Analysis Date = 10/30/16 Pct Recovery = 81% Analysis Date = 10/25/16 Pct Recovery = 81% Analysis Date = 10/25/16 Pct Recovery = 81% Analysis Date = 10/20/16 Pct Recovery = 81% Analysis Date = 10/20/16 Pct Recovery = 81% Analysis Date = 10/15/16 Pct Recovery = 81% Analysis Date = 10/15/16 Pct Recovery = 81% Analysis Date = 10/10/16 Pct Recovery = 81% Analysis Date = 10/10/16 Pct Recovery = 81% Analysis Date = 10/05/16 Pct Recovery = 80% Analysis Date = 10/05/16 Pct Recovery = 80% Analysis Date = 09/30/16 Pct Recovery = 80% Analysis Date = 09/30/16 Pct Recovery = 80% Analysis Date = 09/25/16 Pct Recovery = 80% Analysis Date = 09/25/16 Pct Recovery = 80% Analysis Date = 09/20/16 Pct Recovery = 80% Analysis Date = 09/20/16 Pct Recovery = 80% Analysis Date = 09/15/16 Pct Recovery = 80% Analysis Date = 09/15/16 Pct Recovery = 80% Analysis Date = 09/10/16 Pct Recovery = 80% Analysis Date = 09/10/16 Pct Recovery = 80% Analysis Date = 09/05/16 Pct Recovery = 80% Analysis Date = 09/05/16 Pct Recovery = 80% Analysis Date = 08/31/16 Pct Recovery = 80% Analysis Date = 08/31/16 Pct Recovery = 80% Analysis Date = 08/26/16 Pct Recovery = 79% Analysis Date = 08/26/16 Pct Recovery = 79% Analysis Date = 08/21/16 Pct Recovery = 79% Analysis Date = 08/21/16 Pct Recovery = 79% Analysis Date = 08/16/16 Pct Recovery = 79% Analysis Date = 08/16/16 Pct Recovery = 79% Analysis Date = 08/11/16 Pct Recovery = 79% Analysis Date = 08/11/16 Pct Recovery = 79% Analysis Date = 08/06/16 Pct Recovery = 79% Analysis Date = 08/06/16 Pct Recovery = 79% Analysis Date = 08/01/16 Pct Recovery = 79% Analysis Date = 08/01/16 Pct Recovery = 79% Analysis Date = 07/27/16 Pct Recovery = 79% Analysis Date = 07/27/16 Pct Recovery = 79% Analysis Date = 07/22/16 Pct Recovery = 79% Analysis Date = 07/22/16 Pct Recovery = 79% Analysis Date = 07/17/16 Pct Recovery = 79% Analysis Date = 07/17/16 Pct Recovery = 79% Analysis Date = 07/12/16 Pct Recovery = 79% Analysis Date = 07/12/16 Pct Recovery = 79% Analysis Date = 07/07/16 Pct Recovery = 79% Analysis Date = 07/07/16 Pct Recovery = 79% Analysis Date = 07/02/16 Pct Recovery = 79% Analysis Date = 07/02/16 Pct Recovery = 79% Analysis Date = 06/27/16 Pct Recovery = 79% Analysis Date = 06/27/16 Pct Recovery = 79% Analysis Date = 06/22/16 Pct Recovery = 79% Analysis Date = 06/22/16 Pct Recovery = 79% Analysis Date = 06/17/16 Pct Recovery = 79% Analysis Date = 06/17/16 Pct Recovery = 79% Analysis Date = 06/12/16 Pct Recovery = 79% Analysis Date = 06/12/16 Pct Recovery = 79% Analysis Date = 06/07/16 Pct Recovery = 79% Analysis Date = 06/07/16 Pct Recovery = 79% Analysis Date = 06/02/16 Pct Recovery = 79% Analysis Date = 06/02/16 Pct Recovery = 79% Analysis Date = 05/28/16 Pct Recovery = 79% Analysis Date = 05/28/16 Pct Recovery = 79% Analysis Date = 05/23/16 Pct Recovery = 79% Analysis Date = 05/23/16 Pct Recovery = 79% Analysis Date = 05/18/16 Pct Recovery = 79% Analysis Date = 05/18/16 Pct Recovery = 79% Analysis Date = 05/13/16 Pct Recovery = 79% Analysis Date = 05/13/16 Pct Recovery = 79% Analysis Date = 05/08/16 Pct Recovery = 79% Analysis Date = 05/08/16 Pct Recovery = 79% Analysis Date = 05/03/16 Pct Recovery = 79% Analysis Date = 05/03/16 Pct Recovery = 79% Analysis Date = 04/28/16 Pct Recovery = 79% Analysis Date = 04/28/16 Pct Recovery = 79% Analysis Date = 04/23/16 Pct Recovery = 79% Analysis Date = 04/23/16 Pct Recovery = 79% Analysis Date = 04/18/16 Pct Recovery = 79% Analysis Date = 04/18/16 Pct Recovery = 79% Analysis Date = 04/13/16 Pct Recovery = 79% Analysis Date = 04/13/16 Pct Recovery = 79% Analysis Date = 04/08/16 Pct Recovery = 79% Analysis Date = 04/08/16 Pct Recovery = 79% Analysis Date = 04/03/16 Pct Recovery = 79% Analysis Date = 04/03/16 Pct Recovery = 79% Analysis Date = 03/29/16 Pct Recovery = 79% Analysis Date = 03/29/16 Pct Recovery = 79% Analysis Date = 03/24/16 Pct Recovery = 79% Analysis Date = 03/24/16 Pct Recovery = 79% Analysis Date = 03/19/16 Pct Recovery = 79% Analysis Date = 03/19/16 Pct Recovery = 79% Analysis Date = 03/14/16 Pct Recovery = 79% Analysis Date = 03/14/16 Pct Recovery = 79% Analysis Date = 03/09/16 Pct Recovery = 80% Analysis Date = 03/09/16 Pct Recovery = 80% Analysis Date = 03/04/16 Pct Recovery = 80% Analysis Date = 03/04/16 Pct Recovery = 80% Analysis Date = 02/28/16 Pct Recovery = 80% Analysis Date = 02/28/16 Pct Recovery = 80% Analysis Date = 02/23/16 Pct Recovery = 80% Analysis Date = 02/23/16 Pct Recovery = 80% Analysis Date = 02/18/16 Pct Recovery = 80% Analysis Date = 02/18/16 Pct Recovery = 80% Analysis Date = 02/13/16 Pct Recovery = 80% Analysis Date = 02/13/16 Pct Recovery = 80% Analysis Date = 02/08/16 Pct Recovery = 80% Analysis Date = 02/08/16 Pct Recovery = 80% Analysis Date = 02/03/16 Pct Recovery = 80% Analysis Date = 02/03/16 Pct Recovery = 80% Analysis Date = 01/29/16 Pct Recovery = 80% Analysis Date = 01/29/16 Pct Recovery = 80% Analysis Date = 01/24/16 Pct Recovery = 80% Analysis Date = 01/24/16 Pct Recovery = 80% Analysis Date = 01/19/16 Pct Recovery = 80% Analysis Date = 01/19/16 Pct Recovery = 80% Analysis Date = 01/14/16 Pct Recovery = 80% Analysis Date = 01/14/16 Pct Recovery = 80% Analysis Date = 01/09/16 Pct Recovery = 80% Analysis Date = 01/09/16 Pct Recovery = 80% Analysis Date = 01/04/16 Pct Recovery = 81% Analysis Date = 01/04/16 Pct Recovery = 81% Analysis Date = 12/30/15 Pct Recovery = 81% Analysis Date = 12/30/15 Pct Recovery = 81% Analysis Date = 12/25/15 Pct Recovery = 81% Analysis Date = 12/25/15 Pct Recovery = 81% Analysis Date = 12/20/15 Pct Recovery = 81% Analysis Date = 12/20/15 Pct Recovery = 81% Analysis Date = 12/15/15 Pct Recovery = 81% Analysis Date = 12/15/15 Pct Recovery = 81% Analysis Date = 12/10/15 Pct Recovery = 81% Analysis Date = 12/10/15 Pct Recovery = 81% Analysis Date = 12/05/15 Pct Recovery = 81% Analysis Date = 12/05/15 Pct Recovery = 81% Analysis Date = 11/30/15 Pct Recovery = 81% Analysis Date = 11/30/15 Pct Recovery = 81% Analysis Date = 11/25/15 Pct Recovery = 81% Analysis Date = 11/25/15 Pct Recovery = 81% Analysis Date = 11/20/15 Pct Recovery = 81% Analysis Date = 11/20/15 Pct Recovery = 81% Analysis Date = 11/15/15 Pct Recovery = 81% Analysis Date = 11/15/15 Pct Recovery = 81% Analysis Date = 11/10/15 Pct Recovery = 81% Analysis Date = 11/10/15 Pct Recovery = 81% Analysis Date = 11/05/15 Pct Recovery = 81% Analysis Date = 11/05/15 Pct Recovery = 81% Analysis Date = 10/31/15 Pct Recovery = 81% Analysis Date = 10/31/15 Pct Recovery = 81% Analysis Date = 10/26/15 Pct Recovery = 81% Analysis Date = 10/26/15 Pct Recovery = 81% Analysis Date = 10/21/15 Pct Recovery = 81% Analysis Date = 10/21/15 Pct Recovery = 81% Analysis Date = 10/16/15 Pct Recovery = 81% Analysis Date = 10/16/15 Pct Recovery = 81% Analysis Date = 10/11/15 Pct Recovery = 81% Analysis Date = 10/11/15 Pct Recovery = 81% Analysis Date = 10/06/15 Pct Recovery = 81% Analysis Date = 10/06/15 Pct Recovery = 81% Analysis Date = 10/01/15 Pct Recovery = 81% Analysis Date = 10/01/15 Pct Recovery = 81% Analysis Date = 09/26/15 Pct Recovery = 81% Analysis Date = 09/26/15 Pct Recovery = 81% Analysis Date = 09/21/15 Pct Recovery = 81% Analysis Date = 09/21/15 Pct Recovery = 81% Analysis Date = 09/16/15 Pct Recovery = 81% Analysis Date = 09/16/15 Pct Recovery = 81% Analysis Date = 09/11/15 Pct Recovery = 81% Analysis Date = 09/11/15 Pct Recovery = 81% Analysis Date = 09/05/15 Pct Recovery = 81% Analysis Date = 09/05/15 Pct Recovery = 81% Analysis Date = 08/31/15 Pct Recovery = 81% Analysis Date = 08/31/15 Pct Recovery = 81% Analysis Date = 08/26/15 Pct Recovery = 81% Analysis Date = 08/26/15 Pct Recovery = 81% Analysis Date = 08/21/15 Pct Recovery = 81% Analysis Date = 08/21/15 Pct Recovery = 81% Analysis Date = 08/16/15 Pct Recovery = 81% Analysis Date = 08/16/15 Pct Recovery = 81% Analysis Date = 08/11/15 Pct Recovery = 81% Analysis Date = 08/11/15 Pct Recovery = 81% Analysis Date = 08/06/15 Pct Recovery = 81% Analysis Date = 08/06/15 Pct Recovery = 81% Analysis Date = 08/01/15 Pct Recovery = 81% Analysis Date = 08/01/15 Pct Recovery = 81% Analysis Date = 07/27/15 Pct Recovery = 81% Analysis Date = 07/27/15 Pct Recovery = 81% Analysis Date = 07/22/15 Pct Recovery = 81% Analysis Date = 07/22/15 Pct Recovery = 81% Analysis Date = 07/17/15 Pct Recovery = 81% Analysis Date = 07/17/15 Pct Recovery = 81% Analysis Date = 07/12/15 Pct Recovery = 80% Analysis Date = 07/12/15 Pct Recovery = 80% Analysis Date = 07/07/15 Pct Recovery = 80% Analysis Date = 07/07/15 Pct Recovery = 80% Analysis Date = 07/02/15 Pct Recovery = 80% Analysis Date = 07/02/15 Pct Recovery = 80% Analysis Date = 06/27/15 Pct Recovery = 80% Analysis Date = 06/27/15 Pct Recovery = 80% Analysis Date = 06/22/15 Pct Recovery = 80% Analysis Date = 06/22/15 Pct Recovery = 80% Analysis Date = 06/17/15 Pct Recovery = 80% Analysis Date = 06/17/15 Pct Recovery = 80% Analysis Date = 06/12/15 Pct Recovery = 80% Analysis Date = 06/12/15 Pct Recovery = 80% Analysis Date = 06/07/15 Pct Recovery = 80% Analysis Date = 06/07/15 Pct Recovery = 80% Analysis Date = 06/02/15 Pct Recovery = 80% Analysis Date = 06/02/15 Pct Recovery = 80% Analysis Date = 05/28/15 Pct Recovery = 80% Analysis Date = 05/28/15 Pct Recovery = 80% Analysis Date = 05/23/15 Pct Recovery = 80% Analysis Date = 05/23/15 Pct Recovery = 80% Analysis Date = 05/18/15 Pct Recovery = 79% Analysis Date = 05/18/15 Pct Recovery = 79% Analysis Date = 05/13/15 Pct Recovery = 79% Analysis Date = 05/13/15 Pct Recovery = 79% Analysis Date = 05/08/15 Pct Recovery = 79% Analysis Date = 05/08/15 Pct Recovery = 79% Analysis Date = 05/03/15 Pct Recovery = 79% Analysis Date = 05/03/15 Pct Recovery = 79% Analysis Date = 04/28/15 Pct Recovery = 79% Analysis Date = 04/28/15 Pct Recovery = 79% Analysis Date = 04/23/15 Pct Recovery = 79% Analysis Date = 04/23/15 Pct Recovery = 79% Analysis Date = 04/18/15 Pct Recovery = 79% Analysis Date = 04/18/15 Pct Recovery = 79% Analysis Date = 04/13/15 Pct Recovery = 79% Analysis Date = 04/13/15 Pct Recovery = 79% Analysis Date = 04/08/15 Pct Recovery = 79% Analysis Date = 04/08/15 Pct Recovery = 79% Analysis Date = 04/03/15 Pct Recovery = 79% Analysis Date = 04/03/15 Pct Recovery = 79% Analysis Date = 03/29/15 Pct Recovery = 79% Analysis Date = 03/29/15 Pct Recovery = 79% Analysis Date = 03/24/15 Pct Recovery = 79% Analysis Date = 03/24/15 Pct Recovery = 79% Analysis Date = 03/19/15 Pct Recovery = 78% Analysis Date = 03/19/15 Pct Recovery = 78% Analysis Date = 03/14/15 Pct Recovery = 78% Analysis Date = 03/14/15 Pct Recovery = 78% Analysis Date = 03/09/15 Pct Recovery = 78% Analysis Date = 03/09/15 Pct Recovery = 78% Analysis Date = 03/04/15 Pct Recovery = 78% Analysis Date = 03/04/15 Pct Recovery = 78% Analysis Date = 02/27/15 Pct Recovery = 78% Analysis Date = 02/27/15 Pct Recovery = 78% Analysis Date = 02/22/15 Pct Recovery = 78% Analysis Date = 02/22/15 Pct Recovery = 78% Analysis Date = 02/17/15 Pct Recovery = 78% Analysis Date = 02/17/15 Pct Recovery = 78% Analysis Date = 02/12/15 Pct Recovery = 78% Analysis Date = 02/12/15 Pct Recovery = 78% Analysis Date = 02/07/15 Pct Recovery = 78% Analysis Date = 02/07/15 Pct Recovery = 78% Analysis Date = 02/02/15 Pct Recovery = 78% Analysis Date = 02/02/15 Pct Recovery = 78% Analysis Date = 01/28/15 Pct Recovery = 78% Analysis Date = 01/28/15 Pct Recovery = 78% Analysis Date = 01/23/15 Pct Recovery = 78% Analysis Date = 01/23/15 Pct Recovery = 78% Analysis Date = 01/18/15 Pct Recovery = 77% Analysis Date = 01/18/15 Pct Recovery = 77% Analysis Date = 01/13/15 Pct Recovery = 77% Analysis Date = 01/13/15 Pct Recovery = 77% Analysis Date = 01/08/15 Pct Recovery = 77% Analysis Date = 01/08/15 Pct Recovery = 77% Analysis Date = 01/03/15 Pct Recovery = 77% Analysis Date = 01/03/15 Pct Recovery = 77% Analysis Date = 12/29/14 Pct Recovery = 77% Analysis Date = 12/29/14 Pct Recovery = 77% Analysis Date = 12/24/14 Pct Recovery = 77% Analysis Date = 12/24/14 Pct Recovery = 77% Analysis Date = 12/19/14 Pct Recovery = 77% Analysis Date = 12/19/14 Pct Recovery = 77% Analysis Date = 12/14/14 Pct Recovery = 77% Analysis Date = 12/14/14 Pct Recovery = 77% Analysis Date = 12/09/14 Pct Recovery = 77% Analysis Date = 12/09/14 Pct Recovery = 77% Analysis Date = 12/04/14 Pct Recovery = 77% Analysis Date = 12/04/14 Pct Recovery = 77% Analysis Date = 11/29/14 Pct Recovery = 77% Analysis Date = 11/29/14 Pct Recovery = 77% Analysis Date = 11/24/14 Pct Recovery = 77% Analysis Date = 11/24/14 Pct Recovery = 77% Analysis Date = 11/19/14 Pct Recovery = 76% Analysis Date = 11/19/14 Pct Recovery = 76% Analysis Date = 11/14/14 Pct Recovery = 76% Analysis Date = 11/14/14 Pct Recovery = 76% Analysis Date = 11/09/14 Pct Recovery = 76% Analysis Date = 11/09/14 Pct Recovery = 76% Analysis Date = 11/04/14 Pct Recovery = 76% Analysis Date = 11/04/14 Pct Recovery = 76% Analysis Date = 10/30/14 Pct Recovery = 76% Analysis Date = 10/30/14 Pct Recovery = 76% Analysis Date = 10/25/14 Pct Recovery = 76% Analysis Date = 10/25/14 Pct Recovery = 76% Analysis Date = 10/20/14 Pct Recovery = 76% Analysis Date = 10/20/14 Pct Recovery = 76% Analysis Date = 10/15/14 Pct Recovery = 76% Analysis Date = 10/15/14 Pct Recovery = 76% Analysis Date = 10/10/14 Pct Recovery = 76% Analysis Date = 10/10/14 Pct Recovery = 76% Analysis Date = 10/05/14 Pct Recovery = 76% Analysis Date = 10/05/14 Pct Recovery = 76% Analysis Date = 09/30/14 Pct Recovery = 76% Analysis Date = 09/30/14 Pct Recovery = 76% Analysis Date = 09/25/14 Pct Recovery = 76% Analysis Date = 09/25/14 Pct Recovery = 76% Analysis Date = 09/20/14 Pct Recovery = 75% Analysis Date = 09/20/14 Pct Recovery = 75% Analysis Date = 09/15/14 Pct Recovery = 75% Analysis Date = 09/15/14 Pct Recovery = 75% Analysis Date = 09/10/14 Pct Recovery = 75% Analysis Date = 09/10/14 Pct Recovery = 75% Analysis Date = 09/05/14 Pct Recovery = 75% Analysis Date = 09/05/14 Pct Recovery = 75% Analysis Date = 08/31/14 Pct Recovery = 75% Analysis Date = 08/31/14 Pct Recovery = 75% Analysis Date = 08/26/14 Pct Recovery = 75% Analysis Date = 08/26/14 Pct Recovery = 75% Analysis Date = 08/21/14 Pct Recovery = 75% Analysis Date = 08/21/14 Pct Recovery = 75% Analysis Date = 08/16/14 Pct Recovery = 75% Analysis Date = 08/16/14 Pct Recovery = 75% Analysis Date = 08/11/14 Pct Recovery = 75% Analysis Date = 08/11/14 Pct Recovery = 75% Analysis Date = 08/06/14 Pct Recovery = 75% Analysis Date = 08/06/14 Pct Recovery = 75% Analysis Date = 08/01/14 Pct Recovery = 75% Analysis Date = 08/01/14 Pct Recovery = 75% Analysis Date = 07/27/14 Pct Recovery = 75% Analysis Date = 07/27/14 Pct Recovery = 75% Analysis Date = 07/22/14 Pct Recovery = 74% Analysis Date = 07/22/14 Pct Recovery = 74% Analysis Date = 07/17/14 Pct Recovery = 74% Analysis Date = 07/17/14 Pct Recovery = 74% Analysis Date = 07/12/14 Pct Recovery = 74% Analysis Date = 07/12/14 Pct Recovery = 74% Analysis Date = 07/07/14 Pct Recovery = 74% Analysis Date = 07/07/14 Pct Recovery = 74% Analysis Date = 07/02/14 Pct Recovery = 74% Analysis Date = 07/02/14 Pct Recovery = 74% Analysis Date = 06/27/14 Pct Recovery = 74% Analysis Date = 06/27/14 Pct Recovery = 74% Analysis Date = 06/22/14 Pct Recovery = 74% Analysis Date = 06/22/14 Pct Recovery = 74% Analysis Date = 06/17/14 Pct Recovery = 74% Analysis Date = 06/17/14 Pct Recovery = 74% Analysis Date = 06/12/14 Pct Recovery = 74% Analysis Date = 06/12/14 Pct Recovery = 74% Analysis Date = 06/07/14 Pct Recovery = 74% Analysis Date = 06/07/14 Pct Recovery = 74% Analysis Date = 06/02/14 Pct Recovery = 74% Analysis Date = 06/02/14 Pct Recovery = 74% Analysis Date = 05/28/14 Pct Recovery = 74% Analysis Date = 05/28/14 Pct Recovery = 74% Analysis Date = 05/23/14 Pct Recovery = 74% Analysis Date = 05/23/14 Pct Recovery = 74% Analysis Date = 05/18/14 Pct Recovery = 73% Analysis Date = 05/18/14 Pct Recovery = 73% Analysis Date = 05/13/14 Pct Recovery = 73% Analysis Date = 05/13/14 Pct Recovery = 73% Analysis Date = 05/08/14 Pct Recovery = 73% Analysis Date = 05/08/14 Pct Recovery = 73% Analysis Date = 05/03/14 Pct Recovery = 73% Analysis Date = 05/03/14 Pct Recovery = 73% Analysis Date = 04/28/14 Pct Recovery = 73% Analysis Date = 04/28/14 Pct Recovery = 73% Analysis Date = 04/23/14 Pct Recovery = 73% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
PREDNISOLONE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 2 98% 26% 98% 27%
>= Reporting Level 72 78% 13% 76% 12%
Total 74 79% 14% 77% 12%

Sample Statistics
PREDNISOLONE

Characteristic N % % Basis
Plotted 74 96% Spiked
Estimated Values 19 25% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 77 .  
False Negatives 3 4% 3 out of 77
Not Spiked 38 .  
False Positives 0 0% 0 out of 38

BQS OBSP Determination:
PREDNISONE
METHOD: 2440 , TESTIDCODE: 67467LCM56
Open Data Set

Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 99% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 98% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 100% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 100% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 80 µl & ERA 0406-15-08: 80 µl Pct Recovery = 78% Analysis Date = 11/04/15 SpikeMix = Abs 052215: 80 µl & Abs 050115: 80 µl Pct Recovery = 90% Analysis Date = 01/17/16 SpikeMix = ERA 0406-15-09: 80 µl & ERA 0406-15-07A: 80 µl Pct Recovery = 99% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 80 µl & Abs 051315: 80 µl Pct Recovery = 95% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 81% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 79% Analysis Date = 09/24/16 SpikeMix = Crescent EN160610015: 80 µl & Abs 061416: 80 µl Pct Recovery = 108% Analysis Date = 09/24/16 SpikeMix = Abs 061416: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 102% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 74% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 78% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 88% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 92% Analysis Date = 04/29/15 SpikeMix = ERA 0319-14-05: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 85% Analysis Date = 03/11/15 SpikeMix = ERA 0318-14-02: 15 µl & Abs 041714: 15 µl Pct Recovery = 90% Analysis Date = 02/06/15 SpikeMix = Abs 041814: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 96% Analysis Date = 12/06/14 SpikeMix = ERA 0318-14-02: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 76% Analysis Date = 10/11/14 SpikeMix = ERA 0318-14-02: 60 µl & ERA 0319-14-04: 60 µl Pct Recovery = 71% Analysis Date = 08/21/14 SpikeMix = ERA 0318-14-02: 60 µl & Abs 041714: 60 µl Pct Recovery = 78% Analysis Date = 07/26/14 SpikeMix = ERA 0319-14-05: 60 µl & ERA 0318-14-02: 60 µl Pct Recovery = 92% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 69% Analysis Date = 12/07/14 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 71% Analysis Date = 10/25/14 SpikeMix = Abs 041614: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 83% Analysis Date = 06/22/14 SpikeMix = Abs 041814: 60 µl & Abs 041614: 60 µl Pct Recovery = 114% Analysis Date = 06/11/14 SpikeMix = Abs 041614: 60 µl & Abs 041714: 60 µl Pct Recovery = 99% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 97% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 83% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 80% Analysis Date = 02/23/16 SpikeMix = Abs 052215: 40 µl & Abs 050115: 40 µl Pct Recovery = 78% Analysis Date = 07/31/15 SpikeMix = ERA 0406-15-09: 40 µl & Abs 050115: 40 µl Pct Recovery = 93% Analysis Date = 07/30/15 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 119% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-07A: 40 µl & Abs 051315: 40 µl Pct Recovery = 97% Analysis Date = 11/04/15 SpikeMix = ERA 0406-15-07A: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 84% Analysis Date = 09/10/15 SpikeMix = Abs 052215: 40 µl & ERA 0406-15-07A: 40 µl Pct Recovery = 91% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 87% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 93% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 117% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 112% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 85% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 89% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 85% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 80% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 70% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 74% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 92% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 70% Analysis Date = 12/07/14 SpikeMix = ERA 0318-14-02: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 65% Analysis Date = 11/04/14 SpikeMix = Abs 041814: 8 µl & ERA 0318-14-02: 8 µl Pct Recovery = 78% Analysis Date = 04/30/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 66% Analysis Date = 02/10/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 76% Analysis Date = 10/24/14 SpikeMix = ERA 0319-14-05: 8 µl & Abs 041614: 8 µl Pct Recovery = 94% Analysis Date = 10/10/14 SpikeMix = Abs 041814: 30 µl & ERA 0318-14-02: 30 µl Pct Recovery = 92% Analysis Date = 08/30/14 SpikeMix = ERA 0318-14-02: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 87% Analysis Date = 07/20/14 SpikeMix = ERA 0318-14-02: 30 µl & Abs 041714: 30 µl Pct Recovery = 71% Analysis Date = 09/12/14 SpikeMix = Abs 041614: 30 µl & ERA 0319-14-04: 30 µl Pct Recovery = 82% Analysis Date = 07/13/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 67% Analysis Date = 06/28/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 89% Analysis Date = 05/30/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 100% Analysis Date = 05/17/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 85% Analysis Date = 04/23/14 SpikeMix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.2: 20 µl Pct Recovery = 77% Analysis Date = 11/25/15 SpikeMix = Abs 050115: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 102% Analysis Date = 11/24/15 SpikeMix = ERA 0406-15-09: 20 µl & Abs 050115: 20 µl Pct Recovery = 101% Analysis Date = 08/27/15 SpikeMix = Abs 052215: 20 µl & Abs 050115: 20 µl Pct Recovery = 34% Analysis Date = 08/11/15 SpikeMix = Abs 050115: 20 µl & Abs 051315: 20 µl Pct Recovery = 61% Analysis Date = 07/09/15 SpikeMix = Abs 050115: 20 µl & Abs 052215: 20 µl Pct Recovery = 95% Analysis Date = 06/09/15 SpikeMix = Abs 051315: 20 µl & Abs 050115: 20 µl Pct Recovery = 65% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 57% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 85% Analysis Date = 04/27/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 121% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 94% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 62% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 44% Analysis Date = 11/24/15 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 97% Analysis Date = 09/15/15 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 113% Analysis Date = 01/18/17 Pct Recovery = 94% Analysis Date = 01/13/17 Pct Recovery = 94% Analysis Date = 01/13/17 Pct Recovery = 94% Analysis Date = 01/08/17 Pct Recovery = 94% Analysis Date = 01/08/17 Pct Recovery = 94% Analysis Date = 01/03/17 Pct Recovery = 93% Analysis Date = 01/03/17 Pct Recovery = 93% Analysis Date = 12/29/16 Pct Recovery = 93% Analysis Date = 12/29/16 Pct Recovery = 93% Analysis Date = 12/24/16 Pct Recovery = 93% Analysis Date = 12/24/16 Pct Recovery = 93% Analysis Date = 12/19/16 Pct Recovery = 93% Analysis Date = 12/19/16 Pct Recovery = 93% Analysis Date = 12/14/16 Pct Recovery = 93% Analysis Date = 12/14/16 Pct Recovery = 93% Analysis Date = 12/09/16 Pct Recovery = 92% Analysis Date = 12/09/16 Pct Recovery = 92% Analysis Date = 12/04/16 Pct Recovery = 92% Analysis Date = 12/04/16 Pct Recovery = 92% Analysis Date = 11/29/16 Pct Recovery = 92% Analysis Date = 11/29/16 Pct Recovery = 92% Analysis Date = 11/24/16 Pct Recovery = 92% Analysis Date = 11/24/16 Pct Recovery = 92% Analysis Date = 11/19/16 Pct Recovery = 92% Analysis Date = 11/19/16 Pct Recovery = 92% Analysis Date = 11/14/16 Pct Recovery = 91% Analysis Date = 11/14/16 Pct Recovery = 91% Analysis Date = 11/09/16 Pct Recovery = 91% Analysis Date = 11/09/16 Pct Recovery = 91% Analysis Date = 11/04/16 Pct Recovery = 91% Analysis Date = 11/04/16 Pct Recovery = 91% Analysis Date = 10/30/16 Pct Recovery = 91% Analysis Date = 10/30/16 Pct Recovery = 91% Analysis Date = 10/25/16 Pct Recovery = 91% Analysis Date = 10/25/16 Pct Recovery = 91% Analysis Date = 10/20/16 Pct Recovery = 90% Analysis Date = 10/20/16 Pct Recovery = 90% Analysis Date = 10/15/16 Pct Recovery = 90% Analysis Date = 10/15/16 Pct Recovery = 90% Analysis Date = 10/10/16 Pct Recovery = 90% Analysis Date = 10/10/16 Pct Recovery = 90% Analysis Date = 10/05/16 Pct Recovery = 90% Analysis Date = 10/05/16 Pct Recovery = 90% Analysis Date = 09/30/16 Pct Recovery = 90% Analysis Date = 09/30/16 Pct Recovery = 90% Analysis Date = 09/25/16 Pct Recovery = 89% Analysis Date = 09/25/16 Pct Recovery = 89% Analysis Date = 09/20/16 Pct Recovery = 89% Analysis Date = 09/20/16 Pct Recovery = 89% Analysis Date = 09/15/16 Pct Recovery = 89% Analysis Date = 09/15/16 Pct Recovery = 89% Analysis Date = 09/10/16 Pct Recovery = 89% Analysis Date = 09/10/16 Pct Recovery = 89% Analysis Date = 09/05/16 Pct Recovery = 89% Analysis Date = 09/05/16 Pct Recovery = 89% Analysis Date = 08/31/16 Pct Recovery = 88% Analysis Date = 08/31/16 Pct Recovery = 88% Analysis Date = 08/26/16 Pct Recovery = 88% Analysis Date = 08/26/16 Pct Recovery = 88% Analysis Date = 08/21/16 Pct Recovery = 88% Analysis Date = 08/21/16 Pct Recovery = 88% Analysis Date = 08/16/16 Pct Recovery = 88% Analysis Date = 08/16/16 Pct Recovery = 88% Analysis Date = 08/11/16 Pct Recovery = 88% Analysis Date = 08/11/16 Pct Recovery = 88% Analysis Date = 08/06/16 Pct Recovery = 88% Analysis Date = 08/06/16 Pct Recovery = 88% Analysis Date = 08/01/16 Pct Recovery = 88% Analysis Date = 08/01/16 Pct Recovery = 88% Analysis Date = 07/27/16 Pct Recovery = 88% Analysis Date = 07/27/16 Pct Recovery = 88% Analysis Date = 07/22/16 Pct Recovery = 87% Analysis Date = 07/22/16 Pct Recovery = 87% Analysis Date = 07/17/16 Pct Recovery = 87% Analysis Date = 07/17/16 Pct Recovery = 87% Analysis Date = 07/12/16 Pct Recovery = 87% Analysis Date = 07/12/16 Pct Recovery = 87% Analysis Date = 07/07/16 Pct Recovery = 87% Analysis Date = 07/07/16 Pct Recovery = 87% Analysis Date = 07/02/16 Pct Recovery = 87% Analysis Date = 07/02/16 Pct Recovery = 87% Analysis Date = 06/27/16 Pct Recovery = 87% Analysis Date = 06/27/16 Pct Recovery = 87% Analysis Date = 06/22/16 Pct Recovery = 87% Analysis Date = 06/22/16 Pct Recovery = 87% Analysis Date = 06/17/16 Pct Recovery = 87% Analysis Date = 06/17/16 Pct Recovery = 87% Analysis Date = 06/12/16 Pct Recovery = 87% Analysis Date = 06/12/16 Pct Recovery = 87% Analysis Date = 06/07/16 Pct Recovery = 87% Analysis Date = 06/07/16 Pct Recovery = 87% Analysis Date = 06/02/16 Pct Recovery = 86% Analysis Date = 06/02/16 Pct Recovery = 86% Analysis Date = 05/28/16 Pct Recovery = 86% Analysis Date = 05/28/16 Pct Recovery = 86% Analysis Date = 05/23/16 Pct Recovery = 86% Analysis Date = 05/23/16 Pct Recovery = 86% Analysis Date = 05/18/16 Pct Recovery = 86% Analysis Date = 05/18/16 Pct Recovery = 86% Analysis Date = 05/13/16 Pct Recovery = 86% Analysis Date = 05/13/16 Pct Recovery = 86% Analysis Date = 05/08/16 Pct Recovery = 86% Analysis Date = 05/08/16 Pct Recovery = 86% Analysis Date = 05/03/16 Pct Recovery = 86% Analysis Date = 05/03/16 Pct Recovery = 86% Analysis Date = 04/28/16 Pct Recovery = 86% Analysis Date = 04/28/16 Pct Recovery = 86% Analysis Date = 04/23/16 Pct Recovery = 86% Analysis Date = 04/23/16 Pct Recovery = 86% Analysis Date = 04/18/16 Pct Recovery = 86% Analysis Date = 04/18/16 Pct Recovery = 86% Analysis Date = 04/13/16 Pct Recovery = 86% Analysis Date = 04/13/16 Pct Recovery = 86% Analysis Date = 04/08/16 Pct Recovery = 86% Analysis Date = 04/08/16 Pct Recovery = 86% Analysis Date = 04/03/16 Pct Recovery = 86% Analysis Date = 04/03/16 Pct Recovery = 86% Analysis Date = 03/29/16 Pct Recovery = 86% Analysis Date = 03/29/16 Pct Recovery = 86% Analysis Date = 03/24/16 Pct Recovery = 86% Analysis Date = 03/24/16 Pct Recovery = 86% Analysis Date = 03/19/16 Pct Recovery = 86% Analysis Date = 03/19/16 Pct Recovery = 86% Analysis Date = 03/14/16 Pct Recovery = 86% Analysis Date = 03/14/16 Pct Recovery = 86% Analysis Date = 03/09/16 Pct Recovery = 86% Analysis Date = 03/09/16 Pct Recovery = 86% Analysis Date = 03/04/16 Pct Recovery = 86% Analysis Date = 03/04/16 Pct Recovery = 86% Analysis Date = 02/28/16 Pct Recovery = 86% Analysis Date = 02/28/16 Pct Recovery = 86% Analysis Date = 02/23/16 Pct Recovery = 86% Analysis Date = 02/23/16 Pct Recovery = 86% Analysis Date = 02/18/16 Pct Recovery = 86% Analysis Date = 02/18/16 Pct Recovery = 86% Analysis Date = 02/13/16 Pct Recovery = 86% Analysis Date = 02/13/16 Pct Recovery = 86% Analysis Date = 02/08/16 Pct Recovery = 86% Analysis Date = 02/08/16 Pct Recovery = 86% Analysis Date = 02/03/16 Pct Recovery = 86% Analysis Date = 02/03/16 Pct Recovery = 86% Analysis Date = 01/29/16 Pct Recovery = 86% Analysis Date = 01/29/16 Pct Recovery = 86% Analysis Date = 01/24/16 Pct Recovery = 86% Analysis Date = 01/24/16 Pct Recovery = 86% Analysis Date = 01/19/16 Pct Recovery = 86% Analysis Date = 01/19/16 Pct Recovery = 86% Analysis Date = 01/14/16 Pct Recovery = 86% Analysis Date = 01/14/16 Pct Recovery = 86% Analysis Date = 01/09/16 Pct Recovery = 86% Analysis Date = 01/09/16 Pct Recovery = 86% Analysis Date = 01/04/16 Pct Recovery = 86% Analysis Date = 01/04/16 Pct Recovery = 86% Analysis Date = 12/30/15 Pct Recovery = 86% Analysis Date = 12/30/15 Pct Recovery = 86% Analysis Date = 12/25/15 Pct Recovery = 86% Analysis Date = 12/25/15 Pct Recovery = 86% Analysis Date = 12/20/15 Pct Recovery = 86% Analysis Date = 12/20/15 Pct Recovery = 86% Analysis Date = 12/15/15 Pct Recovery = 86% Analysis Date = 12/15/15 Pct Recovery = 86% Analysis Date = 12/10/15 Pct Recovery = 86% Analysis Date = 12/10/15 Pct Recovery = 86% Analysis Date = 12/05/15 Pct Recovery = 86% Analysis Date = 12/05/15 Pct Recovery = 86% Analysis Date = 11/30/15 Pct Recovery = 86% Analysis Date = 11/30/15 Pct Recovery = 86% Analysis Date = 11/25/15 Pct Recovery = 86% Analysis Date = 11/25/15 Pct Recovery = 86% Analysis Date = 11/20/15 Pct Recovery = 86% Analysis Date = 11/20/15 Pct Recovery = 86% Analysis Date = 11/15/15 Pct Recovery = 86% Analysis Date = 11/15/15 Pct Recovery = 86% Analysis Date = 11/10/15 Pct Recovery = 86% Analysis Date = 11/10/15 Pct Recovery = 86% Analysis Date = 11/05/15 Pct Recovery = 86% Analysis Date = 11/05/15 Pct Recovery = 86% Analysis Date = 10/31/15 Pct Recovery = 86% Analysis Date = 10/31/15 Pct Recovery = 86% Analysis Date = 10/26/15 Pct Recovery = 86% Analysis Date = 10/26/15 Pct Recovery = 86% Analysis Date = 10/21/15 Pct Recovery = 86% Analysis Date = 10/21/15 Pct Recovery = 86% Analysis Date = 10/16/15 Pct Recovery = 86% Analysis Date = 10/16/15 Pct Recovery = 86% Analysis Date = 10/11/15 Pct Recovery = 85% Analysis Date = 10/11/15 Pct Recovery = 85% Analysis Date = 10/06/15 Pct Recovery = 85% Analysis Date = 10/06/15 Pct Recovery = 85% Analysis Date = 10/01/15 Pct Recovery = 85% Analysis Date = 10/01/15 Pct Recovery = 85% Analysis Date = 09/26/15 Pct Recovery = 85% Analysis Date = 09/26/15 Pct Recovery = 85% Analysis Date = 09/21/15 Pct Recovery = 85% Analysis Date = 09/21/15 Pct Recovery = 85% Analysis Date = 09/16/15 Pct Recovery = 85% Analysis Date = 09/16/15 Pct Recovery = 85% Analysis Date = 09/11/15 Pct Recovery = 85% Analysis Date = 09/11/15 Pct Recovery = 85% Analysis Date = 09/05/15 Pct Recovery = 85% Analysis Date = 09/05/15 Pct Recovery = 85% Analysis Date = 08/31/15 Pct Recovery = 85% Analysis Date = 08/31/15 Pct Recovery = 85% Analysis Date = 08/26/15 Pct Recovery = 85% Analysis Date = 08/26/15 Pct Recovery = 85% Analysis Date = 08/21/15 Pct Recovery = 85% Analysis Date = 08/21/15 Pct Recovery = 85% Analysis Date = 08/16/15 Pct Recovery = 85% Analysis Date = 08/16/15 Pct Recovery = 85% Analysis Date = 08/11/15 Pct Recovery = 85% Analysis Date = 08/11/15 Pct Recovery = 85% Analysis Date = 08/06/15 Pct Recovery = 85% Analysis Date = 08/06/15 Pct Recovery = 85% Analysis Date = 08/01/15 Pct Recovery = 84% Analysis Date = 08/01/15 Pct Recovery = 84% Analysis Date = 07/27/15 Pct Recovery = 84% Analysis Date = 07/27/15 Pct Recovery = 84% Analysis Date = 07/22/15 Pct Recovery = 84% Analysis Date = 07/22/15 Pct Recovery = 84% Analysis Date = 07/17/15 Pct Recovery = 84% Analysis Date = 07/17/15 Pct Recovery = 84% Analysis Date = 07/12/15 Pct Recovery = 84% Analysis Date = 07/12/15 Pct Recovery = 84% Analysis Date = 07/07/15 Pct Recovery = 84% Analysis Date = 07/07/15 Pct Recovery = 84% Analysis Date = 07/02/15 Pct Recovery = 84% Analysis Date = 07/02/15 Pct Recovery = 84% Analysis Date = 06/27/15 Pct Recovery = 84% Analysis Date = 06/27/15 Pct Recovery = 84% Analysis Date = 06/22/15 Pct Recovery = 84% Analysis Date = 06/22/15 Pct Recovery = 84% Analysis Date = 06/17/15 Pct Recovery = 84% Analysis Date = 06/17/15 Pct Recovery = 84% Analysis Date = 06/12/15 Pct Recovery = 84% Analysis Date = 06/12/15 Pct Recovery = 84% Analysis Date = 06/07/15 Pct Recovery = 84% Analysis Date = 06/07/15 Pct Recovery = 84% Analysis Date = 06/02/15 Pct Recovery = 84% Analysis Date = 06/02/15 Pct Recovery = 84% Analysis Date = 05/28/15 Pct Recovery = 84% Analysis Date = 05/28/15 Pct Recovery = 84% Analysis Date = 05/23/15 Pct Recovery = 84% Analysis Date = 05/23/15 Pct Recovery = 84% Analysis Date = 05/18/15 Pct Recovery = 83% Analysis Date = 05/18/15 Pct Recovery = 83% Analysis Date = 05/13/15 Pct Recovery = 83% Analysis Date = 05/13/15 Pct Recovery = 83% Analysis Date = 05/08/15 Pct Recovery = 83% Analysis Date = 05/08/15 Pct Recovery = 83% Analysis Date = 05/03/15 Pct Recovery = 83% Analysis Date = 05/03/15 Pct Recovery = 83% Analysis Date = 04/28/15 Pct Recovery = 83% Analysis Date = 04/28/15 Pct Recovery = 83% Analysis Date = 04/23/15 Pct Recovery = 83% Analysis Date = 04/23/15 Pct Recovery = 83% Analysis Date = 04/18/15 Pct Recovery = 83% Analysis Date = 04/18/15 Pct Recovery = 83% Analysis Date = 04/13/15 Pct Recovery = 83% Analysis Date = 04/13/15 Pct Recovery = 83% Analysis Date = 04/08/15 Pct Recovery = 83% Analysis Date = 04/08/15 Pct Recovery = 83% Analysis Date = 04/03/15 Pct Recovery = 83% Analysis Date = 04/03/15 Pct Recovery = 83% Analysis Date = 03/29/15 Pct Recovery = 83% Analysis Date = 03/29/15 Pct Recovery = 83% Analysis Date = 03/24/15 Pct Recovery = 83% Analysis Date = 03/24/15 Pct Recovery = 83% Analysis Date = 03/19/15 Pct Recovery = 83% Analysis Date = 03/19/15 Pct Recovery = 83% Analysis Date = 03/14/15 Pct Recovery = 83% Analysis Date = 03/14/15 Pct Recovery = 83% Analysis Date = 03/09/15 Pct Recovery = 83% Analysis Date = 03/09/15 Pct Recovery = 83% Analysis Date = 03/04/15 Pct Recovery = 83% Analysis Date = 03/04/15 Pct Recovery = 83% Analysis Date = 02/27/15 Pct Recovery = 83% Analysis Date = 02/27/15 Pct Recovery = 83% Analysis Date = 02/22/15 Pct Recovery = 83% Analysis Date = 02/22/15 Pct Recovery = 83% Analysis Date = 02/17/15 Pct Recovery = 83% Analysis Date = 02/17/15 Pct Recovery = 83% Analysis Date = 02/12/15 Pct Recovery = 83% Analysis Date = 02/12/15 Pct Recovery = 83% Analysis Date = 02/07/15 Pct Recovery = 83% Analysis Date = 02/07/15 Pct Recovery = 83% Analysis Date = 02/02/15 Pct Recovery = 83% Analysis Date = 02/02/15 Pct Recovery = 83% Analysis Date = 01/28/15 Pct Recovery = 83% Analysis Date = 01/28/15 Pct Recovery = 83% Analysis Date = 01/23/15 Pct Recovery = 83% Analysis Date = 01/23/15 Pct Recovery = 83% Analysis Date = 01/18/15 Pct Recovery = 83% Analysis Date = 01/18/15 Pct Recovery = 83% Analysis Date = 01/13/15 Pct Recovery = 83% Analysis Date = 01/13/15 Pct Recovery = 83% Analysis Date = 01/08/15 Pct Recovery = 83% Analysis Date = 01/08/15 Pct Recovery = 83% Analysis Date = 01/03/15 Pct Recovery = 83% Analysis Date = 01/03/15 Pct Recovery = 83% Analysis Date = 12/29/14 Pct Recovery = 83% Analysis Date = 12/29/14 Pct Recovery = 83% Analysis Date = 12/24/14 Pct Recovery = 83% Analysis Date = 12/24/14 Pct Recovery = 83% Analysis Date = 12/19/14 Pct Recovery = 83% Analysis Date = 12/19/14 Pct Recovery = 83% Analysis Date = 12/14/14 Pct Recovery = 83% Analysis Date = 12/14/14 Pct Recovery = 83% Analysis Date = 12/09/14 Pct Recovery = 83% Analysis Date = 12/09/14 Pct Recovery = 83% Analysis Date = 12/04/14 Pct Recovery = 83% Analysis Date = 12/04/14 Pct Recovery = 83% Analysis Date = 11/29/14 Pct Recovery = 83% Analysis Date = 11/29/14 Pct Recovery = 83% Analysis Date = 11/24/14 Pct Recovery = 83% Analysis Date = 11/24/14 Pct Recovery = 83% Analysis Date = 11/19/14 Pct Recovery = 83% Analysis Date = 11/19/14 Pct Recovery = 83% Analysis Date = 11/14/14 Pct Recovery = 84% Analysis Date = 11/14/14 Pct Recovery = 84% Analysis Date = 11/09/14 Pct Recovery = 84% Analysis Date = 11/09/14 Pct Recovery = 84% Analysis Date = 11/04/14 Pct Recovery = 84% Analysis Date = 11/04/14 Pct Recovery = 84% Analysis Date = 10/30/14 Pct Recovery = 84% Analysis Date = 10/30/14 Pct Recovery = 84% Analysis Date = 10/25/14 Pct Recovery = 84% Analysis Date = 10/25/14 Pct Recovery = 84% Analysis Date = 10/20/14 Pct Recovery = 84% Analysis Date = 10/20/14 Pct Recovery = 84% Analysis Date = 10/15/14 Pct Recovery = 84% Analysis Date = 10/15/14 Pct Recovery = 84% Analysis Date = 10/10/14 Pct Recovery = 84% Analysis Date = 10/10/14 Pct Recovery = 84% Analysis Date = 10/05/14 Pct Recovery = 84% Analysis Date = 10/05/14 Pct Recovery = 84% Analysis Date = 09/30/14 Pct Recovery = 84% Analysis Date = 09/30/14 Pct Recovery = 84% Analysis Date = 09/25/14 Pct Recovery = 84% Analysis Date = 09/25/14 Pct Recovery = 84% Analysis Date = 09/20/14 Pct Recovery = 84% Analysis Date = 09/20/14 Pct Recovery = 84% Analysis Date = 09/15/14 Pct Recovery = 84% Analysis Date = 09/15/14 Pct Recovery = 84% Analysis Date = 09/10/14 Pct Recovery = 84% Analysis Date = 09/10/14 Pct Recovery = 84% Analysis Date = 09/05/14 Pct Recovery = 84% Analysis Date = 09/05/14 Pct Recovery = 84% Analysis Date = 08/31/14 Pct Recovery = 84% Analysis Date = 08/31/14 Pct Recovery = 84% Analysis Date = 08/26/14 Pct Recovery = 84% Analysis Date = 08/26/14 Pct Recovery = 84% Analysis Date = 08/21/14 Pct Recovery = 84% Analysis Date = 08/21/14 Pct Recovery = 84% Analysis Date = 08/16/14 Pct Recovery = 84% Analysis Date = 08/16/14 Pct Recovery = 84% Analysis Date = 08/11/14 Pct Recovery = 84% Analysis Date = 08/11/14 Pct Recovery = 84% Analysis Date = 08/06/14 Pct Recovery = 85% Analysis Date = 08/06/14 Pct Recovery = 85% Analysis Date = 08/01/14 Pct Recovery = 85% Analysis Date = 08/01/14 Pct Recovery = 85% Analysis Date = 07/27/14 Pct Recovery = 85% Analysis Date = 07/27/14 Pct Recovery = 85% Analysis Date = 07/22/14 Pct Recovery = 85% Analysis Date = 07/22/14 Pct Recovery = 85% Analysis Date = 07/17/14 Pct Recovery = 85% Analysis Date = 07/17/14 Pct Recovery = 85% Analysis Date = 07/12/14 Pct Recovery = 85% Analysis Date = 07/12/14 Pct Recovery = 85% Analysis Date = 07/07/14 Pct Recovery = 85% Analysis Date = 07/07/14 Pct Recovery = 85% Analysis Date = 07/02/14 Pct Recovery = 85% Analysis Date = 07/02/14 Pct Recovery = 85% Analysis Date = 06/27/14 Pct Recovery = 85% Analysis Date = 06/27/14 Pct Recovery = 85% Analysis Date = 06/22/14 Pct Recovery = 85% Analysis Date = 06/22/14 Pct Recovery = 85% Analysis Date = 06/17/14 Pct Recovery = 85% Analysis Date = 06/17/14 Pct Recovery = 85% Analysis Date = 06/12/14 Pct Recovery = 85% Analysis Date = 06/12/14 Pct Recovery = 85% Analysis Date = 06/07/14 Pct Recovery = 85% Analysis Date = 06/07/14 Pct Recovery = 85% Analysis Date = 06/02/14 Pct Recovery = 86% Analysis Date = 06/02/14 Pct Recovery = 86% Analysis Date = 05/28/14 Pct Recovery = 86% Analysis Date = 05/28/14 Pct Recovery = 86% Analysis Date = 05/23/14 Pct Recovery = 86% Analysis Date = 05/23/14 Pct Recovery = 86% Analysis Date = 05/18/14 Pct Recovery = 86% Analysis Date = 05/18/14 Pct Recovery = 86% Analysis Date = 05/13/14 Pct Recovery = 86% Analysis Date = 05/13/14 Pct Recovery = 86% Analysis Date = 05/08/14 Pct Recovery = 86% Analysis Date = 05/08/14 Pct Recovery = 86% Analysis Date = 05/03/14 Pct Recovery = 86% Analysis Date = 05/03/14 Pct Recovery = 86% Analysis Date = 04/28/14 Pct Recovery = 86% Analysis Date = 04/28/14 Pct Recovery = 86% Analysis Date = 04/23/14 Pct Recovery = 86% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
PREDNISONE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 77 86% 16% 87% 14%
Total 77 86% 16% 87% 14%

Sample Statistics
PREDNISONE

Characteristic N % % Basis
Plotted 77 99% Spiked
Estimated Values 35 45% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 78 .  
False Negatives 1 1% 1 out of 78
Not Spiked 37 .  
False Positives 0 0% 0 out of 37

BQS OBSP Determination:
PROMETHAZINE
METHOD: 2440 , TESTIDCODE: 67524LCM56
Open Data Set

Analysis Date = 02/23/16 SpikeMix = Abs 050115: 80 µl & ERA 0406-15-08: 80 µl Pct Recovery = 9% Analysis Date = 11/05/15 SpikeMix = ERA 0406-15-08: 80 µl & Abs 052215: 80 µl Pct Recovery = 11% Analysis Date = 11/24/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 17% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 80 µl & Abs 051315: 80 µl Pct Recovery = 11% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-08: 40 µl & Abs 052215: 40 µl Pct Recovery = 18% Analysis Date = 11/04/15 SpikeMix = ERA 0406-15-07A: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 16% Analysis Date = 04/27/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 33% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 29% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-08: 20 µl & ERA 0406-15-09: 20 µl Pct Recovery = 29% Analysis Date = 09/09/15 SpikeMix = ERA 0406-15-08: 20 µl & Abs 052215: 20 µl Pct Recovery = 28% Analysis Date = 06/26/15 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 24% Analysis Date = 04/26/16 Pct Recovery = 33% Analysis Date = 04/25/16 Pct Recovery = 32% Analysis Date = 04/25/16 Pct Recovery = 32% Analysis Date = 04/23/16 Pct Recovery = 32% Analysis Date = 04/23/16 Pct Recovery = 32% Analysis Date = 04/22/16 Pct Recovery = 31% Analysis Date = 04/22/16 Pct Recovery = 31% Analysis Date = 04/20/16 Pct Recovery = 31% Analysis Date = 04/20/16 Pct Recovery = 31% Analysis Date = 04/19/16 Pct Recovery = 30% Analysis Date = 04/19/16 Pct Recovery = 30% Analysis Date = 04/17/16 Pct Recovery = 30% Analysis Date = 04/17/16 Pct Recovery = 30% Analysis Date = 04/16/16 Pct Recovery = 30% Analysis Date = 04/16/16 Pct Recovery = 30% Analysis Date = 04/14/16 Pct Recovery = 29% Analysis Date = 04/14/16 Pct Recovery = 29% Analysis Date = 04/13/16 Pct Recovery = 29% Analysis Date = 04/13/16 Pct Recovery = 29% Analysis Date = 04/11/16 Pct Recovery = 28% Analysis Date = 04/11/16 Pct Recovery = 28% Analysis Date = 04/10/16 Pct Recovery = 28% Analysis Date = 04/10/16 Pct Recovery = 28% Analysis Date = 04/08/16 Pct Recovery = 27% Analysis Date = 04/08/16 Pct Recovery = 27% Analysis Date = 04/07/16 Pct Recovery = 27% Analysis Date = 04/07/16 Pct Recovery = 27% Analysis Date = 04/05/16 Pct Recovery = 26% Analysis Date = 04/05/16 Pct Recovery = 26% Analysis Date = 04/04/16 Pct Recovery = 26% Analysis Date = 04/04/16 Pct Recovery = 26% Analysis Date = 04/02/16 Pct Recovery = 26% Analysis Date = 04/02/16 Pct Recovery = 26% Analysis Date = 03/31/16 Pct Recovery = 25% Analysis Date = 03/31/16 Pct Recovery = 25% Analysis Date = 03/30/16 Pct Recovery = 25% Analysis Date = 03/30/16 Pct Recovery = 25% Analysis Date = 03/28/16 Pct Recovery = 25% Analysis Date = 03/28/16 Pct Recovery = 25% Analysis Date = 03/27/16 Pct Recovery = 24% Analysis Date = 03/27/16 Pct Recovery = 24% Analysis Date = 03/25/16 Pct Recovery = 24% Analysis Date = 03/25/16 Pct Recovery = 24% Analysis Date = 03/24/16 Pct Recovery = 24% Analysis Date = 03/24/16 Pct Recovery = 24% Analysis Date = 03/22/16 Pct Recovery = 23% Analysis Date = 03/22/16 Pct Recovery = 23% Analysis Date = 03/21/16 Pct Recovery = 23% Analysis Date = 03/21/16 Pct Recovery = 23% Analysis Date = 03/19/16 Pct Recovery = 22% Analysis Date = 03/19/16 Pct Recovery = 22% Analysis Date = 03/18/16 Pct Recovery = 22% Analysis Date = 03/18/16 Pct Recovery = 22% Analysis Date = 03/16/16 Pct Recovery = 22% Analysis Date = 03/16/16 Pct Recovery = 22% Analysis Date = 03/15/16 Pct Recovery = 21% Analysis Date = 03/15/16 Pct Recovery = 21% Analysis Date = 03/13/16 Pct Recovery = 21% Analysis Date = 03/13/16 Pct Recovery = 21% Analysis Date = 03/12/16 Pct Recovery = 21% Analysis Date = 03/12/16 Pct Recovery = 21% Analysis Date = 03/10/16 Pct Recovery = 20% Analysis Date = 03/10/16 Pct Recovery = 20% Analysis Date = 03/09/16 Pct Recovery = 20% Analysis Date = 03/09/16 Pct Recovery = 20% Analysis Date = 03/07/16 Pct Recovery = 19% Analysis Date = 03/07/16 Pct Recovery = 19% Analysis Date = 03/05/16 Pct Recovery = 19% Analysis Date = 03/05/16 Pct Recovery = 19% Analysis Date = 03/04/16 Pct Recovery = 19% Analysis Date = 03/04/16 Pct Recovery = 19% Analysis Date = 03/02/16 Pct Recovery = 18% Analysis Date = 03/02/16 Pct Recovery = 18% Analysis Date = 03/01/16 Pct Recovery = 18% Analysis Date = 03/01/16 Pct Recovery = 18% Analysis Date = 02/28/16 Pct Recovery = 18% Analysis Date = 02/28/16 Pct Recovery = 18% Analysis Date = 02/27/16 Pct Recovery = 18% Analysis Date = 02/27/16 Pct Recovery = 18% Analysis Date = 02/25/16 Pct Recovery = 18% Analysis Date = 02/25/16 Pct Recovery = 18% Analysis Date = 02/24/16 Pct Recovery = 17% Analysis Date = 02/24/16 Pct Recovery = 17% Analysis Date = 02/22/16 Pct Recovery = 17% Analysis Date = 02/22/16 Pct Recovery = 17% Analysis Date = 02/21/16 Pct Recovery = 17% Analysis Date = 02/21/16 Pct Recovery = 17% Analysis Date = 02/19/16 Pct Recovery = 18% Analysis Date = 02/19/16 Pct Recovery = 18% Analysis Date = 02/18/16 Pct Recovery = 18% Analysis Date = 02/18/16 Pct Recovery = 18% Analysis Date = 02/16/16 Pct Recovery = 18% Analysis Date = 02/16/16 Pct Recovery = 18% Analysis Date = 02/15/16 Pct Recovery = 18% Analysis Date = 02/15/16 Pct Recovery = 18% Analysis Date = 02/13/16 Pct Recovery = 18% Analysis Date = 02/13/16 Pct Recovery = 18% Analysis Date = 02/12/16 Pct Recovery = 19% Analysis Date = 02/12/16 Pct Recovery = 19% Analysis Date = 02/10/16 Pct Recovery = 19% Analysis Date = 02/10/16 Pct Recovery = 19% Analysis Date = 02/08/16 Pct Recovery = 19% Analysis Date = 02/08/16 Pct Recovery = 19% Analysis Date = 02/07/16 Pct Recovery = 19% Analysis Date = 02/07/16 Pct Recovery = 19% Analysis Date = 02/05/16 Pct Recovery = 20% Analysis Date = 02/05/16 Pct Recovery = 20% Analysis Date = 02/04/16 Pct Recovery = 20% Analysis Date = 02/04/16 Pct Recovery = 20% Analysis Date = 02/02/16 Pct Recovery = 20% Analysis Date = 02/02/16 Pct Recovery = 20% Analysis Date = 02/01/16 Pct Recovery = 20% Analysis Date = 02/01/16 Pct Recovery = 20% Analysis Date = 01/30/16 Pct Recovery = 21% Analysis Date = 01/30/16 Pct Recovery = 21% Analysis Date = 01/29/16 Pct Recovery = 21% Analysis Date = 01/29/16 Pct Recovery = 21% Analysis Date = 01/27/16 Pct Recovery = 21% Analysis Date = 01/27/16 Pct Recovery = 21% Analysis Date = 01/26/16 Pct Recovery = 21% Analysis Date = 01/26/16 Pct Recovery = 21% Analysis Date = 01/24/16 Pct Recovery = 21% Analysis Date = 01/24/16 Pct Recovery = 21% Analysis Date = 01/23/16 Pct Recovery = 22% Analysis Date = 01/23/16 Pct Recovery = 22% Analysis Date = 01/21/16 Pct Recovery = 22% Analysis Date = 01/21/16 Pct Recovery = 22% Analysis Date = 01/20/16 Pct Recovery = 22% Analysis Date = 01/20/16 Pct Recovery = 22% Analysis Date = 01/18/16 Pct Recovery = 22% Analysis Date = 01/18/16 Pct Recovery = 22% Analysis Date = 01/17/16 Pct Recovery = 23% Analysis Date = 01/17/16 Pct Recovery = 23% Analysis Date = 01/15/16 Pct Recovery = 23% Analysis Date = 01/15/16 Pct Recovery = 23% Analysis Date = 01/13/16 Pct Recovery = 23% Analysis Date = 01/13/16 Pct Recovery = 23% Analysis Date = 01/12/16 Pct Recovery = 23% Analysis Date = 01/12/16 Pct Recovery = 23% Analysis Date = 01/10/16 Pct Recovery = 23% Analysis Date = 01/10/16 Pct Recovery = 23% Analysis Date = 01/09/16 Pct Recovery = 24% Analysis Date = 01/09/16 Pct Recovery = 24% Analysis Date = 01/07/16 Pct Recovery = 24% Analysis Date = 01/07/16 Pct Recovery = 24% Analysis Date = 01/06/16 Pct Recovery = 24% Analysis Date = 01/06/16 Pct Recovery = 24% Analysis Date = 01/04/16 Pct Recovery = 24% Analysis Date = 01/04/16 Pct Recovery = 24% Analysis Date = 01/03/16 Pct Recovery = 25% Analysis Date = 01/03/16 Pct Recovery = 25% Analysis Date = 01/01/16 Pct Recovery = 25% Analysis Date = 01/01/16 Pct Recovery = 25% Analysis Date = 12/31/15 Pct Recovery = 25% Analysis Date = 12/31/15 Pct Recovery = 25% Analysis Date = 12/29/15 Pct Recovery = 25% Analysis Date = 12/29/15 Pct Recovery = 25% Analysis Date = 12/28/15 Pct Recovery = 26% Analysis Date = 12/28/15 Pct Recovery = 26% Analysis Date = 12/26/15 Pct Recovery = 26% Analysis Date = 12/26/15 Pct Recovery = 26% Analysis Date = 12/25/15 Pct Recovery = 26% Analysis Date = 12/25/15 Pct Recovery = 26% Analysis Date = 12/23/15 Pct Recovery = 26% Analysis Date = 12/23/15 Pct Recovery = 26% Analysis Date = 12/22/15 Pct Recovery = 26% Analysis Date = 12/22/15 Pct Recovery = 26% Analysis Date = 12/20/15 Pct Recovery = 27% Analysis Date = 12/20/15 Pct Recovery = 27% Analysis Date = 12/18/15 Pct Recovery = 27% Analysis Date = 12/18/15 Pct Recovery = 27% Analysis Date = 12/17/15 Pct Recovery = 27% Analysis Date = 12/17/15 Pct Recovery = 27% Analysis Date = 12/15/15 Pct Recovery = 27% Analysis Date = 12/15/15 Pct Recovery = 27% Analysis Date = 12/14/15 Pct Recovery = 27% Analysis Date = 12/14/15 Pct Recovery = 27% Analysis Date = 12/12/15 Pct Recovery = 27% Analysis Date = 12/12/15 Pct Recovery = 27% Analysis Date = 12/11/15 Pct Recovery = 26% Analysis Date = 12/11/15 Pct Recovery = 26% Analysis Date = 12/09/15 Pct Recovery = 26% Analysis Date = 12/09/15 Pct Recovery = 26% Analysis Date = 12/08/15 Pct Recovery = 25% Analysis Date = 12/08/15 Pct Recovery = 25% Analysis Date = 12/06/15 Pct Recovery = 25% Analysis Date = 12/06/15 Pct Recovery = 25% Analysis Date = 12/05/15 Pct Recovery = 24% Analysis Date = 12/05/15 Pct Recovery = 24% Analysis Date = 12/03/15 Pct Recovery = 24% Analysis Date = 12/03/15 Pct Recovery = 24% Analysis Date = 12/02/15 Pct Recovery = 23% Analysis Date = 12/02/15 Pct Recovery = 23% Analysis Date = 11/30/15 Pct Recovery = 22% Analysis Date = 11/30/15 Pct Recovery = 22% Analysis Date = 11/29/15 Pct Recovery = 22% Analysis Date = 11/29/15 Pct Recovery = 22% Analysis Date = 11/27/15 Pct Recovery = 21% Analysis Date = 11/27/15 Pct Recovery = 21% Analysis Date = 11/25/15 Pct Recovery = 21% Analysis Date = 11/25/15 Pct Recovery = 21% Analysis Date = 11/24/15 Pct Recovery = 20% Analysis Date = 11/24/15 Pct Recovery = 20% Analysis Date = 11/22/15 Pct Recovery = 20% Analysis Date = 11/22/15 Pct Recovery = 20% Analysis Date = 11/21/15 Pct Recovery = 19% Analysis Date = 11/21/15 Pct Recovery = 19% Analysis Date = 11/19/15 Pct Recovery = 19% Analysis Date = 11/19/15 Pct Recovery = 19% Analysis Date = 11/18/15 Pct Recovery = 19% Analysis Date = 11/18/15 Pct Recovery = 19% Analysis Date = 11/16/15 Pct Recovery = 18% Analysis Date = 11/16/15 Pct Recovery = 18% Analysis Date = 11/15/15 Pct Recovery = 18% Analysis Date = 11/15/15 Pct Recovery = 18% Analysis Date = 11/13/15 Pct Recovery = 17% Analysis Date = 11/13/15 Pct Recovery = 17% Analysis Date = 11/12/15 Pct Recovery = 17% Analysis Date = 11/12/15 Pct Recovery = 17% Analysis Date = 11/10/15 Pct Recovery = 16% Analysis Date = 11/10/15 Pct Recovery = 16% Analysis Date = 11/09/15 Pct Recovery = 16% Analysis Date = 11/09/15 Pct Recovery = 16% Analysis Date = 11/07/15 Pct Recovery = 15% Analysis Date = 11/07/15 Pct Recovery = 15% Analysis Date = 11/06/15 Pct Recovery = 15% Analysis Date = 11/06/15 Pct Recovery = 15% Analysis Date = 11/04/15 Pct Recovery = 15% Analysis Date = 11/04/15 Pct Recovery = 15% Analysis Date = 11/03/15 Pct Recovery = 15% Analysis Date = 11/03/15 Pct Recovery = 15% Analysis Date = 11/01/15 Pct Recovery = 15% Analysis Date = 11/01/15 Pct Recovery = 15% Analysis Date = 10/30/15 Pct Recovery = 15% Analysis Date = 10/30/15 Pct Recovery = 15% Analysis Date = 10/29/15 Pct Recovery = 15% Analysis Date = 10/29/15 Pct Recovery = 15% Analysis Date = 10/27/15 Pct Recovery = 15% Analysis Date = 10/27/15 Pct Recovery = 15% Analysis Date = 10/26/15 Pct Recovery = 16% Analysis Date = 10/26/15 Pct Recovery = 16% Analysis Date = 10/24/15 Pct Recovery = 16% Analysis Date = 10/24/15 Pct Recovery = 16% Analysis Date = 10/23/15 Pct Recovery = 16% Analysis Date = 10/23/15 Pct Recovery = 16% Analysis Date = 10/21/15 Pct Recovery = 16% Analysis Date = 10/21/15 Pct Recovery = 16% Analysis Date = 10/20/15 Pct Recovery = 16% Analysis Date = 10/20/15 Pct Recovery = 16% Analysis Date = 10/18/15 Pct Recovery = 16% Analysis Date = 10/18/15 Pct Recovery = 16% Analysis Date = 10/17/15 Pct Recovery = 17% Analysis Date = 10/17/15 Pct Recovery = 17% Analysis Date = 10/15/15 Pct Recovery = 17% Analysis Date = 10/15/15 Pct Recovery = 17% Analysis Date = 10/14/15 Pct Recovery = 17% Analysis Date = 10/14/15 Pct Recovery = 17% Analysis Date = 10/12/15 Pct Recovery = 17% Analysis Date = 10/12/15 Pct Recovery = 17% Analysis Date = 10/11/15 Pct Recovery = 17% Analysis Date = 10/11/15 Pct Recovery = 17% Analysis Date = 10/09/15 Pct Recovery = 17% Analysis Date = 10/09/15 Pct Recovery = 17% Analysis Date = 10/08/15 Pct Recovery = 18% Analysis Date = 10/08/15 Pct Recovery = 18% Analysis Date = 10/06/15 Pct Recovery = 18% Analysis Date = 10/06/15 Pct Recovery = 18% Analysis Date = 10/04/15 Pct Recovery = 18% Analysis Date = 10/04/15 Pct Recovery = 18% Analysis Date = 10/03/15 Pct Recovery = 18% Analysis Date = 10/03/15 Pct Recovery = 18% Analysis Date = 10/01/15 Pct Recovery = 18% Analysis Date = 10/01/15 Pct Recovery = 18% Analysis Date = 09/30/15 Pct Recovery = 19% Analysis Date = 09/30/15 Pct Recovery = 19% Analysis Date = 09/28/15 Pct Recovery = 19% Analysis Date = 09/28/15 Pct Recovery = 19% Analysis Date = 09/27/15 Pct Recovery = 19% Analysis Date = 09/27/15 Pct Recovery = 19% Analysis Date = 09/25/15 Pct Recovery = 20% Analysis Date = 09/25/15 Pct Recovery = 20% Analysis Date = 09/24/15 Pct Recovery = 20% Analysis Date = 09/24/15 Pct Recovery = 20% Analysis Date = 09/22/15 Pct Recovery = 20% Analysis Date = 09/22/15 Pct Recovery = 20% Analysis Date = 09/21/15 Pct Recovery = 21% Analysis Date = 09/21/15 Pct Recovery = 21% Analysis Date = 09/19/15 Pct Recovery = 21% Analysis Date = 09/19/15 Pct Recovery = 21% Analysis Date = 09/18/15 Pct Recovery = 22% Analysis Date = 09/18/15 Pct Recovery = 22% Analysis Date = 09/16/15 Pct Recovery = 22% Analysis Date = 09/16/15 Pct Recovery = 22% Analysis Date = 09/15/15 Pct Recovery = 22% Analysis Date = 09/15/15 Pct Recovery = 22% Analysis Date = 09/13/15 Pct Recovery = 23% Analysis Date = 09/13/15 Pct Recovery = 23% Analysis Date = 09/12/15 Pct Recovery = 23% Analysis Date = 09/12/15 Pct Recovery = 23% Analysis Date = 09/10/15 Pct Recovery = 23% Analysis Date = 09/10/15 Pct Recovery = 23% Analysis Date = 09/08/15 Pct Recovery = 24% Analysis Date = 09/08/15 Pct Recovery = 24% Analysis Date = 09/07/15 Pct Recovery = 24% Analysis Date = 09/07/15 Pct Recovery = 24% Analysis Date = 09/05/15 Pct Recovery = 24% Analysis Date = 09/05/15 Pct Recovery = 24% Analysis Date = 09/04/15 Pct Recovery = 24% Analysis Date = 09/04/15 Pct Recovery = 24% Analysis Date = 09/02/15 Pct Recovery = 24% Analysis Date = 09/02/15 Pct Recovery = 24% Analysis Date = 09/01/15 Pct Recovery = 24% Analysis Date = 09/01/15 Pct Recovery = 24% Analysis Date = 08/30/15 Pct Recovery = 24% Analysis Date = 08/30/15 Pct Recovery = 24% Analysis Date = 08/29/15 Pct Recovery = 24% Analysis Date = 08/29/15 Pct Recovery = 24% Analysis Date = 08/27/15 Pct Recovery = 24% Analysis Date = 08/27/15 Pct Recovery = 24% Analysis Date = 08/26/15 Pct Recovery = 24% Analysis Date = 08/26/15 Pct Recovery = 24% Analysis Date = 08/24/15 Pct Recovery = 24% Analysis Date = 08/24/15 Pct Recovery = 24% Analysis Date = 08/23/15 Pct Recovery = 24% Analysis Date = 08/23/15 Pct Recovery = 24% Analysis Date = 08/21/15 Pct Recovery = 24% Analysis Date = 08/21/15 Pct Recovery = 24% Analysis Date = 08/20/15 Pct Recovery = 24% Analysis Date = 08/20/15 Pct Recovery = 24% Analysis Date = 08/18/15 Pct Recovery = 24% Analysis Date = 08/18/15 Pct Recovery = 24% Analysis Date = 08/17/15 Pct Recovery = 24% Analysis Date = 08/17/15 Pct Recovery = 24% Analysis Date = 08/15/15 Pct Recovery = 24% Analysis Date = 08/15/15 Pct Recovery = 24% Analysis Date = 08/13/15 Pct Recovery = 24% Analysis Date = 08/13/15 Pct Recovery = 24% Analysis Date = 08/12/15 Pct Recovery = 24% Analysis Date = 08/12/15 Pct Recovery = 24% Analysis Date = 08/10/15 Pct Recovery = 24% Analysis Date = 08/10/15 Pct Recovery = 24% Analysis Date = 08/09/15 Pct Recovery = 24% Analysis Date = 08/09/15 Pct Recovery = 24% Analysis Date = 08/07/15 Pct Recovery = 24% Analysis Date = 08/07/15 Pct Recovery = 24% Analysis Date = 08/06/15 Pct Recovery = 24% Analysis Date = 08/06/15 Pct Recovery = 24% Analysis Date = 08/04/15 Pct Recovery = 24% Analysis Date = 08/04/15 Pct Recovery = 24% Analysis Date = 08/03/15 Pct Recovery = 24% Analysis Date = 08/03/15 Pct Recovery = 24% Analysis Date = 08/01/15 Pct Recovery = 24% Analysis Date = 08/01/15 Pct Recovery = 24% Analysis Date = 07/31/15 Pct Recovery = 24% Analysis Date = 07/31/15 Pct Recovery = 24% Analysis Date = 07/29/15 Pct Recovery = 24% Analysis Date = 07/29/15 Pct Recovery = 24% Analysis Date = 07/28/15 Pct Recovery = 24% Analysis Date = 07/28/15 Pct Recovery = 24% Analysis Date = 07/26/15 Pct Recovery = 24% Analysis Date = 07/26/15 Pct Recovery = 24% Analysis Date = 07/25/15 Pct Recovery = 24% Analysis Date = 07/25/15 Pct Recovery = 24% Analysis Date = 07/23/15 Pct Recovery = 24% Analysis Date = 07/23/15 Pct Recovery = 24% Analysis Date = 07/22/15 Pct Recovery = 24% Analysis Date = 07/22/15 Pct Recovery = 24% Analysis Date = 07/20/15 Pct Recovery = 24% Analysis Date = 07/20/15 Pct Recovery = 24% Analysis Date = 07/18/15 Pct Recovery = 25% Analysis Date = 07/18/15 Pct Recovery = 25% Analysis Date = 07/17/15 Pct Recovery = 25% Analysis Date = 07/17/15 Pct Recovery = 25% Analysis Date = 07/15/15 Pct Recovery = 25% Analysis Date = 07/15/15 Pct Recovery = 25% Analysis Date = 07/14/15 Pct Recovery = 25% Analysis Date = 07/14/15 Pct Recovery = 25% Analysis Date = 07/12/15 Pct Recovery = 25% Analysis Date = 07/12/15 Pct Recovery = 25% Analysis Date = 07/11/15 Pct Recovery = 25% Analysis Date = 07/11/15 Pct Recovery = 25% Analysis Date = 07/09/15 Pct Recovery = 25% Analysis Date = 07/09/15 Pct Recovery = 25% Analysis Date = 07/08/15 Pct Recovery = 25% Analysis Date = 07/08/15 Pct Recovery = 25% Analysis Date = 07/06/15 Pct Recovery = 25% Analysis Date = 07/06/15 Pct Recovery = 25% Analysis Date = 07/05/15 Pct Recovery = 25% Analysis Date = 07/05/15 Pct Recovery = 25% Analysis Date = 07/03/15 Pct Recovery = 25% Analysis Date = 07/03/15 Pct Recovery = 25% Analysis Date = 07/02/15 Pct Recovery = 25% Analysis Date = 07/02/15 Pct Recovery = 25% Analysis Date = 06/30/15 Pct Recovery = 25% Analysis Date = 06/30/15 Pct Recovery = 25% Analysis Date = 06/29/15 Pct Recovery = 25% Analysis Date = 06/29/15 Pct Recovery = 25% Analysis Date = 06/27/15 Pct Recovery = 25% Analysis Date = 06/27/15 Pct Recovery = 25% Analysis Date = 06/26/15 Pct Recovery = 25% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
PROMETHAZINE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 11 20% 8% 18% 13%
Total 11 20% 8% 18% 13%

Sample Statistics
PROMETHAZINE

Characteristic N % % Basis
Plotted 11 14% Spiked
Estimated Values 11 14% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 4 5% Spiked
Spiked 76 .  
False Negatives 61 80% 61 out of 76
Not Spiked 39 .  
False Positives 0 0% 0 out of 39

BQS OBSP Determination:
PROPOXYPHENE
METHOD: 2440 , TESTIDCODE: 68009LCM56
Open Data Set

Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 66% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 68% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 70% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 80% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 80 µl & ERA 0406-15-08: 80 µl Pct Recovery = 67% Analysis Date = 11/05/15 SpikeMix = ERA 0406-15-08: 80 µl & Abs 052215: 80 µl Pct Recovery = 49% Analysis Date = 11/24/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 92% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 80 µl & Abs 051315: 80 µl Pct Recovery = 154% Analysis Date = 10/01/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 119% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 49% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 51% Analysis Date = 09/24/16 SpikeMix = Crescent EN160610015: 80 µl & Abs 061416: 80 µl Pct Recovery = 90% Analysis Date = 09/24/16 SpikeMix = Abs 061416: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 92% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 52% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 59% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 78% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 84% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 51% Analysis Date = 12/07/14 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 68% Analysis Date = 10/25/14 SpikeMix = Abs 041614: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 61% Analysis Date = 06/22/14 SpikeMix = Abs 041814: 60 µl & Abs 041614: 60 µl Pct Recovery = 90% Analysis Date = 06/11/14 SpikeMix = Abs 041614: 60 µl & Abs 041714: 60 µl Pct Recovery = 59% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-08: 40 µl & Abs 052215: 40 µl Pct Recovery = 67% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 64% Analysis Date = 11/04/15 SpikeMix = ERA 0406-15-07A: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 67% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-08: 40 µl & ERA 0406-15-09: 40 µl Pct Recovery = 59% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 52% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 44% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-07A: 40 µl & Abs 051315: 40 µl Pct Recovery = 40% Analysis Date = 07/31/15 SpikeMix = Abs 051315: 40 µl & Abs 052215: 40 µl Pct Recovery = 46% Analysis Date = 07/30/15 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 68% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 56% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 60% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 95% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 105% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 51% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 58% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 57% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 59% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 40% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 55% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 62% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 55% Analysis Date = 04/30/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 55% Analysis Date = 02/10/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 59% Analysis Date = 10/24/14 SpikeMix = ERA 0319-14-05: 8 µl & Abs 041614: 8 µl Pct Recovery = 53% Analysis Date = 09/12/14 SpikeMix = Abs 041614: 30 µl & ERA 0319-14-04: 30 µl Pct Recovery = 46% Analysis Date = 07/13/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 46% Analysis Date = 06/28/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 37% Analysis Date = 05/30/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 59% Analysis Date = 05/17/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 71% Analysis Date = 04/27/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 121% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 57% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-08: 20 µl & ERA 0406-15-09: 20 µl Pct Recovery = 67% Analysis Date = 11/25/15 SpikeMix = Abs 050115: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 80% Analysis Date = 09/15/15 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 68% Analysis Date = 09/09/15 SpikeMix = ERA 0406-15-08: 20 µl & Abs 052215: 20 µl Pct Recovery = 74% Analysis Date = 02/23/16 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 45% Analysis Date = 06/26/15 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 67% Analysis Date = 06/09/15 SpikeMix = Abs 051315: 20 µl & Abs 050115: 20 µl Pct Recovery = 54% Analysis Date = 04/09/16 SpikeMix = Abs 051315: 10 µl & ERA 0406-15-09: 10 µl Pct Recovery = 19% Analysis Date = 01/18/17 Pct Recovery = 67% Analysis Date = 01/14/17 Pct Recovery = 67% Analysis Date = 01/14/17 Pct Recovery = 67% Analysis Date = 01/09/17 Pct Recovery = 67% Analysis Date = 01/09/17 Pct Recovery = 67% Analysis Date = 01/04/17 Pct Recovery = 67% Analysis Date = 01/04/17 Pct Recovery = 67% Analysis Date = 12/30/16 Pct Recovery = 67% Analysis Date = 12/30/16 Pct Recovery = 67% Analysis Date = 12/25/16 Pct Recovery = 67% Analysis Date = 12/25/16 Pct Recovery = 67% Analysis Date = 12/20/16 Pct Recovery = 67% Analysis Date = 12/20/16 Pct Recovery = 67% Analysis Date = 12/15/16 Pct Recovery = 67% Analysis Date = 12/15/16 Pct Recovery = 67% Analysis Date = 12/10/16 Pct Recovery = 67% Analysis Date = 12/10/16 Pct Recovery = 67% Analysis Date = 12/05/16 Pct Recovery = 67% Analysis Date = 12/05/16 Pct Recovery = 67% Analysis Date = 12/01/16 Pct Recovery = 66% Analysis Date = 12/01/16 Pct Recovery = 66% Analysis Date = 11/26/16 Pct Recovery = 66% Analysis Date = 11/26/16 Pct Recovery = 66% Analysis Date = 11/21/16 Pct Recovery = 66% Analysis Date = 11/21/16 Pct Recovery = 66% Analysis Date = 11/16/16 Pct Recovery = 66% Analysis Date = 11/16/16 Pct Recovery = 66% Analysis Date = 11/11/16 Pct Recovery = 66% Analysis Date = 11/11/16 Pct Recovery = 66% Analysis Date = 11/06/16 Pct Recovery = 66% Analysis Date = 11/06/16 Pct Recovery = 66% Analysis Date = 11/01/16 Pct Recovery = 66% Analysis Date = 11/01/16 Pct Recovery = 66% Analysis Date = 10/27/16 Pct Recovery = 66% Analysis Date = 10/27/16 Pct Recovery = 66% Analysis Date = 10/22/16 Pct Recovery = 66% Analysis Date = 10/22/16 Pct Recovery = 66% Analysis Date = 10/18/16 Pct Recovery = 66% Analysis Date = 10/18/16 Pct Recovery = 66% Analysis Date = 10/13/16 Pct Recovery = 66% Analysis Date = 10/13/16 Pct Recovery = 66% Analysis Date = 10/08/16 Pct Recovery = 66% Analysis Date = 10/08/16 Pct Recovery = 66% Analysis Date = 10/03/16 Pct Recovery = 66% Analysis Date = 10/03/16 Pct Recovery = 66% Analysis Date = 09/28/16 Pct Recovery = 66% Analysis Date = 09/28/16 Pct Recovery = 66% Analysis Date = 09/23/16 Pct Recovery = 66% Analysis Date = 09/23/16 Pct Recovery = 66% Analysis Date = 09/18/16 Pct Recovery = 65% Analysis Date = 09/18/16 Pct Recovery = 65% Analysis Date = 09/13/16 Pct Recovery = 65% Analysis Date = 09/13/16 Pct Recovery = 65% Analysis Date = 09/08/16 Pct Recovery = 65% Analysis Date = 09/08/16 Pct Recovery = 65% Analysis Date = 09/04/16 Pct Recovery = 65% Analysis Date = 09/04/16 Pct Recovery = 65% Analysis Date = 08/30/16 Pct Recovery = 65% Analysis Date = 08/30/16 Pct Recovery = 65% Analysis Date = 08/25/16 Pct Recovery = 65% Analysis Date = 08/25/16 Pct Recovery = 65% Analysis Date = 08/20/16 Pct Recovery = 65% Analysis Date = 08/20/16 Pct Recovery = 65% Analysis Date = 08/15/16 Pct Recovery = 65% Analysis Date = 08/15/16 Pct Recovery = 65% Analysis Date = 08/10/16 Pct Recovery = 65% Analysis Date = 08/10/16 Pct Recovery = 65% Analysis Date = 08/05/16 Pct Recovery = 65% Analysis Date = 08/05/16 Pct Recovery = 65% Analysis Date = 07/31/16 Pct Recovery = 65% Analysis Date = 07/31/16 Pct Recovery = 65% Analysis Date = 07/26/16 Pct Recovery = 64% Analysis Date = 07/26/16 Pct Recovery = 64% Analysis Date = 07/22/16 Pct Recovery = 64% Analysis Date = 07/22/16 Pct Recovery = 64% Analysis Date = 07/17/16 Pct Recovery = 64% Analysis Date = 07/17/16 Pct Recovery = 64% Analysis Date = 07/12/16 Pct Recovery = 64% Analysis Date = 07/12/16 Pct Recovery = 64% Analysis Date = 07/07/16 Pct Recovery = 64% Analysis Date = 07/07/16 Pct Recovery = 64% Analysis Date = 07/02/16 Pct Recovery = 64% Analysis Date = 07/02/16 Pct Recovery = 64% Analysis Date = 06/27/16 Pct Recovery = 64% Analysis Date = 06/27/16 Pct Recovery = 64% Analysis Date = 06/22/16 Pct Recovery = 64% Analysis Date = 06/22/16 Pct Recovery = 64% Analysis Date = 06/17/16 Pct Recovery = 64% Analysis Date = 06/17/16 Pct Recovery = 64% Analysis Date = 06/12/16 Pct Recovery = 63% Analysis Date = 06/12/16 Pct Recovery = 63% Analysis Date = 06/08/16 Pct Recovery = 63% Analysis Date = 06/08/16 Pct Recovery = 63% Analysis Date = 06/03/16 Pct Recovery = 63% Analysis Date = 06/03/16 Pct Recovery = 63% Analysis Date = 05/29/16 Pct Recovery = 63% Analysis Date = 05/29/16 Pct Recovery = 63% Analysis Date = 05/24/16 Pct Recovery = 63% Analysis Date = 05/24/16 Pct Recovery = 63% Analysis Date = 05/19/16 Pct Recovery = 63% Analysis Date = 05/19/16 Pct Recovery = 63% Analysis Date = 05/14/16 Pct Recovery = 63% Analysis Date = 05/14/16 Pct Recovery = 63% Analysis Date = 05/09/16 Pct Recovery = 63% Analysis Date = 05/09/16 Pct Recovery = 63% Analysis Date = 05/04/16 Pct Recovery = 62% Analysis Date = 05/04/16 Pct Recovery = 62% Analysis Date = 04/29/16 Pct Recovery = 62% Analysis Date = 04/29/16 Pct Recovery = 62% Analysis Date = 04/25/16 Pct Recovery = 62% Analysis Date = 04/25/16 Pct Recovery = 62% Analysis Date = 04/20/16 Pct Recovery = 62% Analysis Date = 04/20/16 Pct Recovery = 62% Analysis Date = 04/15/16 Pct Recovery = 63% Analysis Date = 04/15/16 Pct Recovery = 63% Analysis Date = 04/10/16 Pct Recovery = 63% Analysis Date = 04/10/16 Pct Recovery = 63% Analysis Date = 04/05/16 Pct Recovery = 63% Analysis Date = 04/05/16 Pct Recovery = 63% Analysis Date = 03/31/16 Pct Recovery = 63% Analysis Date = 03/31/16 Pct Recovery = 63% Analysis Date = 03/26/16 Pct Recovery = 63% Analysis Date = 03/26/16 Pct Recovery = 63% Analysis Date = 03/21/16 Pct Recovery = 64% Analysis Date = 03/21/16 Pct Recovery = 64% Analysis Date = 03/16/16 Pct Recovery = 64% Analysis Date = 03/16/16 Pct Recovery = 64% Analysis Date = 03/12/16 Pct Recovery = 64% Analysis Date = 03/12/16 Pct Recovery = 64% Analysis Date = 03/07/16 Pct Recovery = 64% Analysis Date = 03/07/16 Pct Recovery = 64% Analysis Date = 03/02/16 Pct Recovery = 64% Analysis Date = 03/02/16 Pct Recovery = 64% Analysis Date = 02/26/16 Pct Recovery = 64% Analysis Date = 02/26/16 Pct Recovery = 64% Analysis Date = 02/21/16 Pct Recovery = 65% Analysis Date = 02/21/16 Pct Recovery = 65% Analysis Date = 02/16/16 Pct Recovery = 65% Analysis Date = 02/16/16 Pct Recovery = 65% Analysis Date = 02/11/16 Pct Recovery = 65% Analysis Date = 02/11/16 Pct Recovery = 65% Analysis Date = 02/06/16 Pct Recovery = 65% Analysis Date = 02/06/16 Pct Recovery = 65% Analysis Date = 02/01/16 Pct Recovery = 66% Analysis Date = 02/01/16 Pct Recovery = 66% Analysis Date = 01/28/16 Pct Recovery = 66% Analysis Date = 01/28/16 Pct Recovery = 66% Analysis Date = 01/23/16 Pct Recovery = 66% Analysis Date = 01/23/16 Pct Recovery = 66% Analysis Date = 01/18/16 Pct Recovery = 66% Analysis Date = 01/18/16 Pct Recovery = 66% Analysis Date = 01/13/16 Pct Recovery = 66% Analysis Date = 01/13/16 Pct Recovery = 66% Analysis Date = 01/08/16 Pct Recovery = 67% Analysis Date = 01/08/16 Pct Recovery = 67% Analysis Date = 01/03/16 Pct Recovery = 67% Analysis Date = 01/03/16 Pct Recovery = 67% Analysis Date = 12/29/15 Pct Recovery = 67% Analysis Date = 12/29/15 Pct Recovery = 67% Analysis Date = 12/24/15 Pct Recovery = 67% Analysis Date = 12/24/15 Pct Recovery = 67% Analysis Date = 12/19/15 Pct Recovery = 68% Analysis Date = 12/19/15 Pct Recovery = 68% Analysis Date = 12/15/15 Pct Recovery = 68% Analysis Date = 12/15/15 Pct Recovery = 68% Analysis Date = 12/10/15 Pct Recovery = 68% Analysis Date = 12/10/15 Pct Recovery = 68% Analysis Date = 12/05/15 Pct Recovery = 68% Analysis Date = 12/05/15 Pct Recovery = 68% Analysis Date = 11/30/15 Pct Recovery = 68% Analysis Date = 11/30/15 Pct Recovery = 68% Analysis Date = 11/25/15 Pct Recovery = 69% Analysis Date = 11/25/15 Pct Recovery = 69% Analysis Date = 11/20/15 Pct Recovery = 69% Analysis Date = 11/20/15 Pct Recovery = 69% Analysis Date = 11/15/15 Pct Recovery = 69% Analysis Date = 11/15/15 Pct Recovery = 69% Analysis Date = 11/10/15 Pct Recovery = 69% Analysis Date = 11/10/15 Pct Recovery = 69% Analysis Date = 11/05/15 Pct Recovery = 70% Analysis Date = 11/05/15 Pct Recovery = 70% Analysis Date = 11/01/15 Pct Recovery = 70% Analysis Date = 11/01/15 Pct Recovery = 70% Analysis Date = 10/27/15 Pct Recovery = 70% Analysis Date = 10/27/15 Pct Recovery = 70% Analysis Date = 10/22/15 Pct Recovery = 69% Analysis Date = 10/22/15 Pct Recovery = 69% Analysis Date = 10/17/15 Pct Recovery = 69% Analysis Date = 10/17/15 Pct Recovery = 69% Analysis Date = 10/12/15 Pct Recovery = 69% Analysis Date = 10/12/15 Pct Recovery = 69% Analysis Date = 10/07/15 Pct Recovery = 69% Analysis Date = 10/07/15 Pct Recovery = 69% Analysis Date = 10/02/15 Pct Recovery = 69% Analysis Date = 10/02/15 Pct Recovery = 69% Analysis Date = 09/27/15 Pct Recovery = 69% Analysis Date = 09/27/15 Pct Recovery = 69% Analysis Date = 09/22/15 Pct Recovery = 69% Analysis Date = 09/22/15 Pct Recovery = 69% Analysis Date = 09/17/15 Pct Recovery = 69% Analysis Date = 09/17/15 Pct Recovery = 69% Analysis Date = 09/13/15 Pct Recovery = 69% Analysis Date = 09/13/15 Pct Recovery = 69% Analysis Date = 09/08/15 Pct Recovery = 69% Analysis Date = 09/08/15 Pct Recovery = 69% Analysis Date = 09/03/15 Pct Recovery = 68% Analysis Date = 09/03/15 Pct Recovery = 68% Analysis Date = 08/29/15 Pct Recovery = 68% Analysis Date = 08/29/15 Pct Recovery = 68% Analysis Date = 08/24/15 Pct Recovery = 68% Analysis Date = 08/24/15 Pct Recovery = 68% Analysis Date = 08/19/15 Pct Recovery = 68% Analysis Date = 08/19/15 Pct Recovery = 68% Analysis Date = 08/14/15 Pct Recovery = 68% Analysis Date = 08/14/15 Pct Recovery = 68% Analysis Date = 08/09/15 Pct Recovery = 68% Analysis Date = 08/09/15 Pct Recovery = 68% Analysis Date = 08/04/15 Pct Recovery = 68% Analysis Date = 08/04/15 Pct Recovery = 68% Analysis Date = 07/31/15 Pct Recovery = 68% Analysis Date = 07/31/15 Pct Recovery = 68% Analysis Date = 07/26/15 Pct Recovery = 68% Analysis Date = 07/26/15 Pct Recovery = 68% Analysis Date = 07/21/15 Pct Recovery = 67% Analysis Date = 07/21/15 Pct Recovery = 67% Analysis Date = 07/16/15 Pct Recovery = 67% Analysis Date = 07/16/15 Pct Recovery = 67% Analysis Date = 07/11/15 Pct Recovery = 67% Analysis Date = 07/11/15 Pct Recovery = 67% Analysis Date = 07/06/15 Pct Recovery = 67% Analysis Date = 07/06/15 Pct Recovery = 67% Analysis Date = 07/01/15 Pct Recovery = 67% Analysis Date = 07/01/15 Pct Recovery = 67% Analysis Date = 06/26/15 Pct Recovery = 67% Analysis Date = 06/26/15 Pct Recovery = 67% Analysis Date = 06/21/15 Pct Recovery = 67% Analysis Date = 06/21/15 Pct Recovery = 67% Analysis Date = 06/17/15 Pct Recovery = 66% Analysis Date = 06/17/15 Pct Recovery = 66% Analysis Date = 06/12/15 Pct Recovery = 66% Analysis Date = 06/12/15 Pct Recovery = 66% Analysis Date = 06/07/15 Pct Recovery = 66% Analysis Date = 06/07/15 Pct Recovery = 66% Analysis Date = 06/02/15 Pct Recovery = 66% Analysis Date = 06/02/15 Pct Recovery = 66% Analysis Date = 05/28/15 Pct Recovery = 66% Analysis Date = 05/28/15 Pct Recovery = 66% Analysis Date = 05/23/15 Pct Recovery = 66% Analysis Date = 05/23/15 Pct Recovery = 66% Analysis Date = 05/18/15 Pct Recovery = 66% Analysis Date = 05/18/15 Pct Recovery = 66% Analysis Date = 05/13/15 Pct Recovery = 66% Analysis Date = 05/13/15 Pct Recovery = 66% Analysis Date = 05/08/15 Pct Recovery = 65% Analysis Date = 05/08/15 Pct Recovery = 65% Analysis Date = 05/04/15 Pct Recovery = 65% Analysis Date = 05/04/15 Pct Recovery = 65% Analysis Date = 04/29/15 Pct Recovery = 65% Analysis Date = 04/29/15 Pct Recovery = 65% Analysis Date = 04/24/15 Pct Recovery = 65% Analysis Date = 04/24/15 Pct Recovery = 65% Analysis Date = 04/19/15 Pct Recovery = 65% Analysis Date = 04/19/15 Pct Recovery = 65% Analysis Date = 04/14/15 Pct Recovery = 65% Analysis Date = 04/14/15 Pct Recovery = 65% Analysis Date = 04/09/15 Pct Recovery = 65% Analysis Date = 04/09/15 Pct Recovery = 65% Analysis Date = 04/04/15 Pct Recovery = 64% Analysis Date = 04/04/15 Pct Recovery = 64% Analysis Date = 03/30/15 Pct Recovery = 64% Analysis Date = 03/30/15 Pct Recovery = 64% Analysis Date = 03/25/15 Pct Recovery = 64% Analysis Date = 03/25/15 Pct Recovery = 64% Analysis Date = 03/21/15 Pct Recovery = 64% Analysis Date = 03/21/15 Pct Recovery = 64% Analysis Date = 03/16/15 Pct Recovery = 64% Analysis Date = 03/16/15 Pct Recovery = 64% Analysis Date = 03/11/15 Pct Recovery = 64% Analysis Date = 03/11/15 Pct Recovery = 64% Analysis Date = 03/06/15 Pct Recovery = 64% Analysis Date = 03/06/15 Pct Recovery = 64% Analysis Date = 03/01/15 Pct Recovery = 63% Analysis Date = 03/01/15 Pct Recovery = 63% Analysis Date = 02/24/15 Pct Recovery = 63% Analysis Date = 02/24/15 Pct Recovery = 63% Analysis Date = 02/19/15 Pct Recovery = 63% Analysis Date = 02/19/15 Pct Recovery = 63% Analysis Date = 02/14/15 Pct Recovery = 63% Analysis Date = 02/14/15 Pct Recovery = 63% Analysis Date = 02/09/15 Pct Recovery = 63% Analysis Date = 02/09/15 Pct Recovery = 63% Analysis Date = 02/05/15 Pct Recovery = 63% Analysis Date = 02/05/15 Pct Recovery = 63% Analysis Date = 01/31/15 Pct Recovery = 63% Analysis Date = 01/31/15 Pct Recovery = 63% Analysis Date = 01/26/15 Pct Recovery = 63% Analysis Date = 01/26/15 Pct Recovery = 63% Analysis Date = 01/21/15 Pct Recovery = 62% Analysis Date = 01/21/15 Pct Recovery = 62% Analysis Date = 01/16/15 Pct Recovery = 62% Analysis Date = 01/16/15 Pct Recovery = 62% Analysis Date = 01/11/15 Pct Recovery = 62% Analysis Date = 01/11/15 Pct Recovery = 62% Analysis Date = 01/06/15 Pct Recovery = 62% Analysis Date = 01/06/15 Pct Recovery = 62% Analysis Date = 01/01/15 Pct Recovery = 62% Analysis Date = 01/01/15 Pct Recovery = 62% Analysis Date = 12/27/14 Pct Recovery = 62% Analysis Date = 12/27/14 Pct Recovery = 62% Analysis Date = 12/23/14 Pct Recovery = 62% Analysis Date = 12/23/14 Pct Recovery = 62% Analysis Date = 12/18/14 Pct Recovery = 62% Analysis Date = 12/18/14 Pct Recovery = 62% Analysis Date = 12/13/14 Pct Recovery = 61% Analysis Date = 12/13/14 Pct Recovery = 61% Analysis Date = 12/08/14 Pct Recovery = 61% Analysis Date = 12/08/14 Pct Recovery = 61% Analysis Date = 12/03/14 Pct Recovery = 61% Analysis Date = 12/03/14 Pct Recovery = 61% Analysis Date = 11/28/14 Pct Recovery = 61% Analysis Date = 11/28/14 Pct Recovery = 61% Analysis Date = 11/23/14 Pct Recovery = 61% Analysis Date = 11/23/14 Pct Recovery = 61% Analysis Date = 11/18/14 Pct Recovery = 61% Analysis Date = 11/18/14 Pct Recovery = 61% Analysis Date = 11/13/14 Pct Recovery = 61% Analysis Date = 11/13/14 Pct Recovery = 61% Analysis Date = 11/09/14 Pct Recovery = 61% Analysis Date = 11/09/14 Pct Recovery = 61% Analysis Date = 11/04/14 Pct Recovery = 60% Analysis Date = 11/04/14 Pct Recovery = 60% Analysis Date = 10/30/14 Pct Recovery = 60% Analysis Date = 10/30/14 Pct Recovery = 60% Analysis Date = 10/25/14 Pct Recovery = 60% Analysis Date = 10/25/14 Pct Recovery = 60% Analysis Date = 10/20/14 Pct Recovery = 60% Analysis Date = 10/20/14 Pct Recovery = 60% Analysis Date = 10/15/14 Pct Recovery = 60% Analysis Date = 10/15/14 Pct Recovery = 60% Analysis Date = 10/10/14 Pct Recovery = 60% Analysis Date = 10/10/14 Pct Recovery = 60% Analysis Date = 10/05/14 Pct Recovery = 60% Analysis Date = 10/05/14 Pct Recovery = 60% Analysis Date = 09/30/14 Pct Recovery = 60% Analysis Date = 09/30/14 Pct Recovery = 60% Analysis Date = 09/26/14 Pct Recovery = 59% Analysis Date = 09/26/14 Pct Recovery = 59% Analysis Date = 09/21/14 Pct Recovery = 59% Analysis Date = 09/21/14 Pct Recovery = 59% Analysis Date = 09/16/14 Pct Recovery = 59% Analysis Date = 09/16/14 Pct Recovery = 59% Analysis Date = 09/11/14 Pct Recovery = 59% Analysis Date = 09/11/14 Pct Recovery = 59% Analysis Date = 09/06/14 Pct Recovery = 59% Analysis Date = 09/06/14 Pct Recovery = 59% Analysis Date = 09/01/14 Pct Recovery = 59% Analysis Date = 09/01/14 Pct Recovery = 59% Analysis Date = 08/27/14 Pct Recovery = 59% Analysis Date = 08/27/14 Pct Recovery = 59% Analysis Date = 08/22/14 Pct Recovery = 59% Analysis Date = 08/22/14 Pct Recovery = 59% Analysis Date = 08/17/14 Pct Recovery = 58% Analysis Date = 08/17/14 Pct Recovery = 58% Analysis Date = 08/13/14 Pct Recovery = 58% Analysis Date = 08/13/14 Pct Recovery = 58% Analysis Date = 08/08/14 Pct Recovery = 58% Analysis Date = 08/08/14 Pct Recovery = 58% Analysis Date = 08/03/14 Pct Recovery = 58% Analysis Date = 08/03/14 Pct Recovery = 58% Analysis Date = 07/29/14 Pct Recovery = 58% Analysis Date = 07/29/14 Pct Recovery = 58% Analysis Date = 07/24/14 Pct Recovery = 58% Analysis Date = 07/24/14 Pct Recovery = 58% Analysis Date = 07/19/14 Pct Recovery = 58% Analysis Date = 07/19/14 Pct Recovery = 58% Analysis Date = 07/14/14 Pct Recovery = 58% Analysis Date = 07/14/14 Pct Recovery = 58% Analysis Date = 07/09/14 Pct Recovery = 57% Analysis Date = 07/09/14 Pct Recovery = 57% Analysis Date = 07/04/14 Pct Recovery = 57% Analysis Date = 07/04/14 Pct Recovery = 57% Analysis Date = 06/30/14 Pct Recovery = 57% Analysis Date = 06/30/14 Pct Recovery = 57% Analysis Date = 06/25/14 Pct Recovery = 57% Analysis Date = 06/25/14 Pct Recovery = 57% Analysis Date = 06/20/14 Pct Recovery = 57% Analysis Date = 06/20/14 Pct Recovery = 57% Analysis Date = 06/15/14 Pct Recovery = 57% Analysis Date = 06/15/14 Pct Recovery = 57% Analysis Date = 06/10/14 Pct Recovery = 57% Analysis Date = 06/10/14 Pct Recovery = 57% Analysis Date = 06/05/14 Pct Recovery = 57% Analysis Date = 06/05/14 Pct Recovery = 57% Analysis Date = 05/31/14 Pct Recovery = 56% Analysis Date = 05/31/14 Pct Recovery = 56% Analysis Date = 05/26/14 Pct Recovery = 56% Analysis Date = 05/26/14 Pct Recovery = 56% Analysis Date = 05/21/14 Pct Recovery = 56% Analysis Date = 05/21/14 Pct Recovery = 56% Analysis Date = 05/17/14 Pct Recovery = 56% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
PROPOXYPHENE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 1 19% . 19% 0%
>= Reporting Level 60 66% 21% 60% 13%
Total 61 65% 22% 59% 13%

Sample Statistics
PROPOXYPHENE

Characteristic N % % Basis
Plotted 61 97% Spiked
Estimated Values 25 40% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 1 2% Spiked
Spiked 63 .  
False Negatives 1 2% 1 out of 63
Not Spiked 52 .  
False Positives 0 0% 0 out of 52

BQS OBSP Determination:
PROPRANOLOL
METHOD: 2440 , TESTIDCODE: 67516LCM56
Open Data Set

Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 83% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 83% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 79% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 81% Analysis Date = 11/05/15 SpikeMix = ERA 0406-15-08: 80 µl & Abs 052215: 80 µl Pct Recovery = 76% Analysis Date = 11/04/15 SpikeMix = Abs 052215: 80 µl & Abs 050115: 80 µl Pct Recovery = 68% Analysis Date = 01/17/16 SpikeMix = ERA 0406-15-09: 80 µl & ERA 0406-15-07A: 80 µl Pct Recovery = 77% Analysis Date = 11/24/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 73% Analysis Date = 10/01/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 84% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 77% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 75% Analysis Date = 09/24/16 SpikeMix = Crescent EN160610015: 80 µl & Abs 061416: 80 µl Pct Recovery = 80% Analysis Date = 09/24/16 SpikeMix = Abs 061416: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 83% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 69% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 73% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 79% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 80% Analysis Date = 05/07/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 80% Analysis Date = 03/11/15 SpikeMix = ERA 0318-14-02: 15 µl & Abs 041714: 15 µl Pct Recovery = 76% Analysis Date = 01/16/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 76% Analysis Date = 12/06/14 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 64% Analysis Date = 08/21/14 SpikeMix = ERA 0318-14-02: 60 µl & Abs 041714: 60 µl Pct Recovery = 57% Analysis Date = 07/12/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 64% Analysis Date = 06/11/14 SpikeMix = Abs 041614: 60 µl & Abs 041714: 60 µl Pct Recovery = 63% Analysis Date = 05/21/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 69% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-04: 15 µl & Abs 041814: 15 µl Pct Recovery = 57% Analysis Date = 12/06/14 SpikeMix = ERA 0318-14-02: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 66% Analysis Date = 10/25/14 SpikeMix = Abs 041614: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 75% Analysis Date = 10/11/14 SpikeMix = ERA 0318-14-02: 60 µl & ERA 0319-14-04: 60 µl Pct Recovery = 64% Analysis Date = 08/28/14 SpikeMix = ERA 0319-14-04: 60 µl & ERA 0319-14-05: 60 µl Pct Recovery = 60% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-08: 40 µl & Abs 052215: 40 µl Pct Recovery = 60% Analysis Date = 02/23/16 SpikeMix = Abs 052215: 40 µl & Abs 050115: 40 µl Pct Recovery = 74% Analysis Date = 09/10/15 SpikeMix = Abs 052215: 40 µl & ERA 0406-15-07A: 40 µl Pct Recovery = 84% Analysis Date = 07/31/15 SpikeMix = Abs 051315: 40 µl & Abs 052215: 40 µl Pct Recovery = 62% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-08: 40 µl & ERA 0406-15-09: 40 µl Pct Recovery = 68% Analysis Date = 07/31/15 SpikeMix = ERA 0406-15-09: 40 µl & Abs 050115: 40 µl Pct Recovery = 83% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 78% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 71% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 88% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 88% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 70% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 73% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 70% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 73% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 50% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 62% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 61% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 63% Analysis Date = 11/04/14 SpikeMix = Abs 041714: 8 µl & ERA 0319-14-05: 8 µl Pct Recovery = 57% Analysis Date = 04/30/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 67% Analysis Date = 04/10/15 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 65% Analysis Date = 02/10/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 67% Analysis Date = 12/07/14 SpikeMix = ERA 0318-14-02: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 71% Analysis Date = 10/11/14 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 60% Analysis Date = 10/10/14 SpikeMix = Abs 041714: 30 µl & Abs 041814: 30 µl Pct Recovery = 60% Analysis Date = 07/20/14 SpikeMix = ERA 0318-14-02: 30 µl & Abs 041714: 30 µl Pct Recovery = 52% Analysis Date = 06/28/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 64% Analysis Date = 05/17/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 72% Analysis Date = 09/12/14 SpikeMix = Abs 041614: 30 µl & ERA 0319-14-04: 30 µl Pct Recovery = 55% Analysis Date = 08/16/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 60% Analysis Date = 07/13/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 53% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 48% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 42% Analysis Date = 02/23/16 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 72% Analysis Date = 11/24/15 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 72% Analysis Date = 09/09/15 SpikeMix = ERA 0406-15-08: 20 µl & Abs 052215: 20 µl Pct Recovery = 78% Analysis Date = 08/27/15 SpikeMix = Abs 052215: 20 µl & Abs 050115: 20 µl Pct Recovery = 65% Analysis Date = 07/09/15 SpikeMix = Abs 050115: 20 µl & Abs 052215: 20 µl Pct Recovery = 69% Analysis Date = 06/26/15 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 65% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 71% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 56% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-08: 20 µl & ERA 0406-15-09: 20 µl Pct Recovery = 65% Analysis Date = 11/24/15 SpikeMix = ERA 0406-15-09: 20 µl & Abs 050115: 20 µl Pct Recovery = 70% Analysis Date = 04/09/16 SpikeMix = Abs 051315: 10 µl & ERA 0406-15-09: 10 µl Pct Recovery = 49% Analysis Date = 01/18/17 Pct Recovery = 80% Analysis Date = 01/14/17 Pct Recovery = 80% Analysis Date = 01/14/17 Pct Recovery = 80% Analysis Date = 01/09/17 Pct Recovery = 79% Analysis Date = 01/09/17 Pct Recovery = 79% Analysis Date = 01/04/17 Pct Recovery = 79% Analysis Date = 01/04/17 Pct Recovery = 79% Analysis Date = 12/30/16 Pct Recovery = 79% Analysis Date = 12/30/16 Pct Recovery = 79% Analysis Date = 12/25/16 Pct Recovery = 79% Analysis Date = 12/25/16 Pct Recovery = 79% Analysis Date = 12/20/16 Pct Recovery = 78% Analysis Date = 12/20/16 Pct Recovery = 78% Analysis Date = 12/15/16 Pct Recovery = 78% Analysis Date = 12/15/16 Pct Recovery = 78% Analysis Date = 12/10/16 Pct Recovery = 78% Analysis Date = 12/10/16 Pct Recovery = 78% Analysis Date = 12/05/16 Pct Recovery = 77% Analysis Date = 12/05/16 Pct Recovery = 77% Analysis Date = 12/01/16 Pct Recovery = 77% Analysis Date = 12/01/16 Pct Recovery = 77% Analysis Date = 11/26/16 Pct Recovery = 77% Analysis Date = 11/26/16 Pct Recovery = 77% Analysis Date = 11/21/16 Pct Recovery = 76% Analysis Date = 11/21/16 Pct Recovery = 76% Analysis Date = 11/16/16 Pct Recovery = 76% Analysis Date = 11/16/16 Pct Recovery = 76% Analysis Date = 11/11/16 Pct Recovery = 76% Analysis Date = 11/11/16 Pct Recovery = 76% Analysis Date = 11/06/16 Pct Recovery = 76% Analysis Date = 11/06/16 Pct Recovery = 76% Analysis Date = 11/01/16 Pct Recovery = 75% Analysis Date = 11/01/16 Pct Recovery = 75% Analysis Date = 10/27/16 Pct Recovery = 75% Analysis Date = 10/27/16 Pct Recovery = 75% Analysis Date = 10/22/16 Pct Recovery = 75% Analysis Date = 10/22/16 Pct Recovery = 75% Analysis Date = 10/18/16 Pct Recovery = 74% Analysis Date = 10/18/16 Pct Recovery = 74% Analysis Date = 10/13/16 Pct Recovery = 74% Analysis Date = 10/13/16 Pct Recovery = 74% Analysis Date = 10/08/16 Pct Recovery = 74% Analysis Date = 10/08/16 Pct Recovery = 74% Analysis Date = 10/03/16 Pct Recovery = 74% Analysis Date = 10/03/16 Pct Recovery = 74% Analysis Date = 09/28/16 Pct Recovery = 73% Analysis Date = 09/28/16 Pct Recovery = 73% Analysis Date = 09/23/16 Pct Recovery = 73% Analysis Date = 09/23/16 Pct Recovery = 73% Analysis Date = 09/18/16 Pct Recovery = 73% Analysis Date = 09/18/16 Pct Recovery = 73% Analysis Date = 09/13/16 Pct Recovery = 73% Analysis Date = 09/13/16 Pct Recovery = 73% Analysis Date = 09/08/16 Pct Recovery = 72% Analysis Date = 09/08/16 Pct Recovery = 72% Analysis Date = 09/04/16 Pct Recovery = 72% Analysis Date = 09/04/16 Pct Recovery = 72% Analysis Date = 08/30/16 Pct Recovery = 72% Analysis Date = 08/30/16 Pct Recovery = 72% Analysis Date = 08/25/16 Pct Recovery = 72% Analysis Date = 08/25/16 Pct Recovery = 72% Analysis Date = 08/20/16 Pct Recovery = 71% Analysis Date = 08/20/16 Pct Recovery = 71% Analysis Date = 08/15/16 Pct Recovery = 71% Analysis Date = 08/15/16 Pct Recovery = 71% Analysis Date = 08/10/16 Pct Recovery = 71% Analysis Date = 08/10/16 Pct Recovery = 71% Analysis Date = 08/05/16 Pct Recovery = 71% Analysis Date = 08/05/16 Pct Recovery = 71% Analysis Date = 07/31/16 Pct Recovery = 70% Analysis Date = 07/31/16 Pct Recovery = 70% Analysis Date = 07/26/16 Pct Recovery = 70% Analysis Date = 07/26/16 Pct Recovery = 70% Analysis Date = 07/22/16 Pct Recovery = 70% Analysis Date = 07/22/16 Pct Recovery = 70% Analysis Date = 07/17/16 Pct Recovery = 70% Analysis Date = 07/17/16 Pct Recovery = 70% Analysis Date = 07/12/16 Pct Recovery = 70% Analysis Date = 07/12/16 Pct Recovery = 70% Analysis Date = 07/07/16 Pct Recovery = 70% Analysis Date = 07/07/16 Pct Recovery = 70% Analysis Date = 07/02/16 Pct Recovery = 69% Analysis Date = 07/02/16 Pct Recovery = 69% Analysis Date = 06/27/16 Pct Recovery = 69% Analysis Date = 06/27/16 Pct Recovery = 69% Analysis Date = 06/22/16 Pct Recovery = 69% Analysis Date = 06/22/16 Pct Recovery = 69% Analysis Date = 06/17/16 Pct Recovery = 69% Analysis Date = 06/17/16 Pct Recovery = 69% Analysis Date = 06/12/16 Pct Recovery = 69% Analysis Date = 06/12/16 Pct Recovery = 69% Analysis Date = 06/08/16 Pct Recovery = 69% Analysis Date = 06/08/16 Pct Recovery = 69% Analysis Date = 06/03/16 Pct Recovery = 69% Analysis Date = 06/03/16 Pct Recovery = 69% Analysis Date = 05/29/16 Pct Recovery = 68% Analysis Date = 05/29/16 Pct Recovery = 68% Analysis Date = 05/24/16 Pct Recovery = 68% Analysis Date = 05/24/16 Pct Recovery = 68% Analysis Date = 05/19/16 Pct Recovery = 68% Analysis Date = 05/19/16 Pct Recovery = 68% Analysis Date = 05/14/16 Pct Recovery = 68% Analysis Date = 05/14/16 Pct Recovery = 68% Analysis Date = 05/09/16 Pct Recovery = 68% Analysis Date = 05/09/16 Pct Recovery = 68% Analysis Date = 05/04/16 Pct Recovery = 68% Analysis Date = 05/04/16 Pct Recovery = 68% Analysis Date = 04/29/16 Pct Recovery = 68% Analysis Date = 04/29/16 Pct Recovery = 68% Analysis Date = 04/25/16 Pct Recovery = 67% Analysis Date = 04/25/16 Pct Recovery = 67% Analysis Date = 04/20/16 Pct Recovery = 67% Analysis Date = 04/20/16 Pct Recovery = 67% Analysis Date = 04/15/16 Pct Recovery = 67% Analysis Date = 04/15/16 Pct Recovery = 67% Analysis Date = 04/10/16 Pct Recovery = 67% Analysis Date = 04/10/16 Pct Recovery = 67% Analysis Date = 04/05/16 Pct Recovery = 67% Analysis Date = 04/05/16 Pct Recovery = 67% Analysis Date = 03/31/16 Pct Recovery = 67% Analysis Date = 03/31/16 Pct Recovery = 67% Analysis Date = 03/26/16 Pct Recovery = 67% Analysis Date = 03/26/16 Pct Recovery = 67% Analysis Date = 03/21/16 Pct Recovery = 67% Analysis Date = 03/21/16 Pct Recovery = 67% Analysis Date = 03/16/16 Pct Recovery = 67% Analysis Date = 03/16/16 Pct Recovery = 67% Analysis Date = 03/12/16 Pct Recovery = 67% Analysis Date = 03/12/16 Pct Recovery = 67% Analysis Date = 03/07/16 Pct Recovery = 67% Analysis Date = 03/07/16 Pct Recovery = 67% Analysis Date = 03/02/16 Pct Recovery = 67% Analysis Date = 03/02/16 Pct Recovery = 67% Analysis Date = 02/26/16 Pct Recovery = 67% Analysis Date = 02/26/16 Pct Recovery = 67% Analysis Date = 02/21/16 Pct Recovery = 68% Analysis Date = 02/21/16 Pct Recovery = 68% Analysis Date = 02/16/16 Pct Recovery = 68% Analysis Date = 02/16/16 Pct Recovery = 68% Analysis Date = 02/11/16 Pct Recovery = 68% Analysis Date = 02/11/16 Pct Recovery = 68% Analysis Date = 02/06/16 Pct Recovery = 68% Analysis Date = 02/06/16 Pct Recovery = 68% Analysis Date = 02/01/16 Pct Recovery = 68% Analysis Date = 02/01/16 Pct Recovery = 68% Analysis Date = 01/28/16 Pct Recovery = 68% Analysis Date = 01/28/16 Pct Recovery = 68% Analysis Date = 01/23/16 Pct Recovery = 68% Analysis Date = 01/23/16 Pct Recovery = 68% Analysis Date = 01/18/16 Pct Recovery = 68% Analysis Date = 01/18/16 Pct Recovery = 68% Analysis Date = 01/13/16 Pct Recovery = 68% Analysis Date = 01/13/16 Pct Recovery = 68% Analysis Date = 01/08/16 Pct Recovery = 68% Analysis Date = 01/08/16 Pct Recovery = 68% Analysis Date = 01/03/16 Pct Recovery = 68% Analysis Date = 01/03/16 Pct Recovery = 68% Analysis Date = 12/29/15 Pct Recovery = 68% Analysis Date = 12/29/15 Pct Recovery = 68% Analysis Date = 12/24/15 Pct Recovery = 68% Analysis Date = 12/24/15 Pct Recovery = 68% Analysis Date = 12/19/15 Pct Recovery = 69% Analysis Date = 12/19/15 Pct Recovery = 69% Analysis Date = 12/15/15 Pct Recovery = 69% Analysis Date = 12/15/15 Pct Recovery = 69% Analysis Date = 12/10/15 Pct Recovery = 69% Analysis Date = 12/10/15 Pct Recovery = 69% Analysis Date = 12/05/15 Pct Recovery = 69% Analysis Date = 12/05/15 Pct Recovery = 69% Analysis Date = 11/30/15 Pct Recovery = 69% Analysis Date = 11/30/15 Pct Recovery = 69% Analysis Date = 11/25/15 Pct Recovery = 69% Analysis Date = 11/25/15 Pct Recovery = 69% Analysis Date = 11/20/15 Pct Recovery = 69% Analysis Date = 11/20/15 Pct Recovery = 69% Analysis Date = 11/15/15 Pct Recovery = 69% Analysis Date = 11/15/15 Pct Recovery = 69% Analysis Date = 11/10/15 Pct Recovery = 69% Analysis Date = 11/10/15 Pct Recovery = 69% Analysis Date = 11/05/15 Pct Recovery = 69% Analysis Date = 11/05/15 Pct Recovery = 69% Analysis Date = 11/01/15 Pct Recovery = 70% Analysis Date = 11/01/15 Pct Recovery = 70% Analysis Date = 10/27/15 Pct Recovery = 70% Analysis Date = 10/27/15 Pct Recovery = 70% Analysis Date = 10/22/15 Pct Recovery = 70% Analysis Date = 10/22/15 Pct Recovery = 70% Analysis Date = 10/17/15 Pct Recovery = 70% Analysis Date = 10/17/15 Pct Recovery = 70% Analysis Date = 10/12/15 Pct Recovery = 70% Analysis Date = 10/12/15 Pct Recovery = 70% Analysis Date = 10/07/15 Pct Recovery = 70% Analysis Date = 10/07/15 Pct Recovery = 70% Analysis Date = 10/02/15 Pct Recovery = 70% Analysis Date = 10/02/15 Pct Recovery = 70% Analysis Date = 09/27/15 Pct Recovery = 70% Analysis Date = 09/27/15 Pct Recovery = 70% Analysis Date = 09/22/15 Pct Recovery = 70% Analysis Date = 09/22/15 Pct Recovery = 70% Analysis Date = 09/17/15 Pct Recovery = 70% Analysis Date = 09/17/15 Pct Recovery = 70% Analysis Date = 09/13/15 Pct Recovery = 70% Analysis Date = 09/13/15 Pct Recovery = 70% Analysis Date = 09/08/15 Pct Recovery = 70% Analysis Date = 09/08/15 Pct Recovery = 70% Analysis Date = 09/03/15 Pct Recovery = 70% Analysis Date = 09/03/15 Pct Recovery = 70% Analysis Date = 08/29/15 Pct Recovery = 70% Analysis Date = 08/29/15 Pct Recovery = 70% Analysis Date = 08/24/15 Pct Recovery = 70% Analysis Date = 08/24/15 Pct Recovery = 70% Analysis Date = 08/19/15 Pct Recovery = 70% Analysis Date = 08/19/15 Pct Recovery = 70% Analysis Date = 08/14/15 Pct Recovery = 70% Analysis Date = 08/14/15 Pct Recovery = 70% Analysis Date = 08/09/15 Pct Recovery = 70% Analysis Date = 08/09/15 Pct Recovery = 70% Analysis Date = 08/04/15 Pct Recovery = 70% Analysis Date = 08/04/15 Pct Recovery = 70% Analysis Date = 07/31/15 Pct Recovery = 70% Analysis Date = 07/31/15 Pct Recovery = 70% Analysis Date = 07/26/15 Pct Recovery = 70% Analysis Date = 07/26/15 Pct Recovery = 70% Analysis Date = 07/21/15 Pct Recovery = 70% Analysis Date = 07/21/15 Pct Recovery = 70% Analysis Date = 07/16/15 Pct Recovery = 70% Analysis Date = 07/16/15 Pct Recovery = 70% Analysis Date = 07/11/15 Pct Recovery = 70% Analysis Date = 07/11/15 Pct Recovery = 70% Analysis Date = 07/06/15 Pct Recovery = 70% Analysis Date = 07/06/15 Pct Recovery = 70% Analysis Date = 07/01/15 Pct Recovery = 70% Analysis Date = 07/01/15 Pct Recovery = 70% Analysis Date = 06/26/15 Pct Recovery = 70% Analysis Date = 06/26/15 Pct Recovery = 70% Analysis Date = 06/21/15 Pct Recovery = 70% Analysis Date = 06/21/15 Pct Recovery = 70% Analysis Date = 06/17/15 Pct Recovery = 70% Analysis Date = 06/17/15 Pct Recovery = 70% Analysis Date = 06/12/15 Pct Recovery = 70% Analysis Date = 06/12/15 Pct Recovery = 70% Analysis Date = 06/07/15 Pct Recovery = 70% Analysis Date = 06/07/15 Pct Recovery = 70% Analysis Date = 06/02/15 Pct Recovery = 70% Analysis Date = 06/02/15 Pct Recovery = 70% Analysis Date = 05/28/15 Pct Recovery = 70% Analysis Date = 05/28/15 Pct Recovery = 70% Analysis Date = 05/23/15 Pct Recovery = 70% Analysis Date = 05/23/15 Pct Recovery = 70% Analysis Date = 05/18/15 Pct Recovery = 69% Analysis Date = 05/18/15 Pct Recovery = 69% Analysis Date = 05/13/15 Pct Recovery = 69% Analysis Date = 05/13/15 Pct Recovery = 69% Analysis Date = 05/08/15 Pct Recovery = 69% Analysis Date = 05/08/15 Pct Recovery = 69% Analysis Date = 05/04/15 Pct Recovery = 69% Analysis Date = 05/04/15 Pct Recovery = 69% Analysis Date = 04/29/15 Pct Recovery = 69% Analysis Date = 04/29/15 Pct Recovery = 69% Analysis Date = 04/24/15 Pct Recovery = 69% Analysis Date = 04/24/15 Pct Recovery = 69% Analysis Date = 04/19/15 Pct Recovery = 69% Analysis Date = 04/19/15 Pct Recovery = 69% Analysis Date = 04/14/15 Pct Recovery = 69% Analysis Date = 04/14/15 Pct Recovery = 69% Analysis Date = 04/09/15 Pct Recovery = 69% Analysis Date = 04/09/15 Pct Recovery = 69% Analysis Date = 04/04/15 Pct Recovery = 69% Analysis Date = 04/04/15 Pct Recovery = 69% Analysis Date = 03/30/15 Pct Recovery = 68% Analysis Date = 03/30/15 Pct Recovery = 68% Analysis Date = 03/25/15 Pct Recovery = 68% Analysis Date = 03/25/15 Pct Recovery = 68% Analysis Date = 03/21/15 Pct Recovery = 68% Analysis Date = 03/21/15 Pct Recovery = 68% Analysis Date = 03/16/15 Pct Recovery = 68% Analysis Date = 03/16/15 Pct Recovery = 68% Analysis Date = 03/11/15 Pct Recovery = 68% Analysis Date = 03/11/15 Pct Recovery = 68% Analysis Date = 03/06/15 Pct Recovery = 68% Analysis Date = 03/06/15 Pct Recovery = 68% Analysis Date = 03/01/15 Pct Recovery = 68% Analysis Date = 03/01/15 Pct Recovery = 68% Analysis Date = 02/24/15 Pct Recovery = 68% Analysis Date = 02/24/15 Pct Recovery = 68% Analysis Date = 02/19/15 Pct Recovery = 67% Analysis Date = 02/19/15 Pct Recovery = 67% Analysis Date = 02/14/15 Pct Recovery = 67% Analysis Date = 02/14/15 Pct Recovery = 67% Analysis Date = 02/09/15 Pct Recovery = 67% Analysis Date = 02/09/15 Pct Recovery = 67% Analysis Date = 02/05/15 Pct Recovery = 67% Analysis Date = 02/05/15 Pct Recovery = 67% Analysis Date = 01/31/15 Pct Recovery = 67% Analysis Date = 01/31/15 Pct Recovery = 67% Analysis Date = 01/26/15 Pct Recovery = 67% Analysis Date = 01/26/15 Pct Recovery = 67% Analysis Date = 01/21/15 Pct Recovery = 67% Analysis Date = 01/21/15 Pct Recovery = 67% Analysis Date = 01/16/15 Pct Recovery = 66% Analysis Date = 01/16/15 Pct Recovery = 66% Analysis Date = 01/11/15 Pct Recovery = 66% Analysis Date = 01/11/15 Pct Recovery = 66% Analysis Date = 01/06/15 Pct Recovery = 66% Analysis Date = 01/06/15 Pct Recovery = 66% Analysis Date = 01/01/15 Pct Recovery = 66% Analysis Date = 01/01/15 Pct Recovery = 66% Analysis Date = 12/27/14 Pct Recovery = 66% Analysis Date = 12/27/14 Pct Recovery = 66% Analysis Date = 12/23/14 Pct Recovery = 66% Analysis Date = 12/23/14 Pct Recovery = 66% Analysis Date = 12/18/14 Pct Recovery = 66% Analysis Date = 12/18/14 Pct Recovery = 66% Analysis Date = 12/13/14 Pct Recovery = 65% Analysis Date = 12/13/14 Pct Recovery = 65% Analysis Date = 12/08/14 Pct Recovery = 65% Analysis Date = 12/08/14 Pct Recovery = 65% Analysis Date = 12/03/14 Pct Recovery = 65% Analysis Date = 12/03/14 Pct Recovery = 65% Analysis Date = 11/28/14 Pct Recovery = 65% Analysis Date = 11/28/14 Pct Recovery = 65% Analysis Date = 11/23/14 Pct Recovery = 65% Analysis Date = 11/23/14 Pct Recovery = 65% Analysis Date = 11/18/14 Pct Recovery = 65% Analysis Date = 11/18/14 Pct Recovery = 65% Analysis Date = 11/13/14 Pct Recovery = 65% Analysis Date = 11/13/14 Pct Recovery = 65% Analysis Date = 11/09/14 Pct Recovery = 65% Analysis Date = 11/09/14 Pct Recovery = 65% Analysis Date = 11/04/14 Pct Recovery = 64% Analysis Date = 11/04/14 Pct Recovery = 64% Analysis Date = 10/30/14 Pct Recovery = 64% Analysis Date = 10/30/14 Pct Recovery = 64% Analysis Date = 10/25/14 Pct Recovery = 64% Analysis Date = 10/25/14 Pct Recovery = 64% Analysis Date = 10/20/14 Pct Recovery = 64% Analysis Date = 10/20/14 Pct Recovery = 64% Analysis Date = 10/15/14 Pct Recovery = 64% Analysis Date = 10/15/14 Pct Recovery = 64% Analysis Date = 10/10/14 Pct Recovery = 64% Analysis Date = 10/10/14 Pct Recovery = 64% Analysis Date = 10/05/14 Pct Recovery = 64% Analysis Date = 10/05/14 Pct Recovery = 64% Analysis Date = 09/30/14 Pct Recovery = 64% Analysis Date = 09/30/14 Pct Recovery = 64% Analysis Date = 09/26/14 Pct Recovery = 63% Analysis Date = 09/26/14 Pct Recovery = 63% Analysis Date = 09/21/14 Pct Recovery = 63% Analysis Date = 09/21/14 Pct Recovery = 63% Analysis Date = 09/16/14 Pct Recovery = 63% Analysis Date = 09/16/14 Pct Recovery = 63% Analysis Date = 09/11/14 Pct Recovery = 63% Analysis Date = 09/11/14 Pct Recovery = 63% Analysis Date = 09/06/14 Pct Recovery = 63% Analysis Date = 09/06/14 Pct Recovery = 63% Analysis Date = 09/01/14 Pct Recovery = 63% Analysis Date = 09/01/14 Pct Recovery = 63% Analysis Date = 08/27/14 Pct Recovery = 63% Analysis Date = 08/27/14 Pct Recovery = 63% Analysis Date = 08/22/14 Pct Recovery = 63% Analysis Date = 08/22/14 Pct Recovery = 63% Analysis Date = 08/17/14 Pct Recovery = 62% Analysis Date = 08/17/14 Pct Recovery = 62% Analysis Date = 08/13/14 Pct Recovery = 62% Analysis Date = 08/13/14 Pct Recovery = 62% Analysis Date = 08/08/14 Pct Recovery = 62% Analysis Date = 08/08/14 Pct Recovery = 62% Analysis Date = 08/03/14 Pct Recovery = 62% Analysis Date = 08/03/14 Pct Recovery = 62% Analysis Date = 07/29/14 Pct Recovery = 62% Analysis Date = 07/29/14 Pct Recovery = 62% Analysis Date = 07/24/14 Pct Recovery = 62% Analysis Date = 07/24/14 Pct Recovery = 62% Analysis Date = 07/19/14 Pct Recovery = 62% Analysis Date = 07/19/14 Pct Recovery = 62% Analysis Date = 07/14/14 Pct Recovery = 62% Analysis Date = 07/14/14 Pct Recovery = 62% Analysis Date = 07/09/14 Pct Recovery = 61% Analysis Date = 07/09/14 Pct Recovery = 61% Analysis Date = 07/04/14 Pct Recovery = 61% Analysis Date = 07/04/14 Pct Recovery = 61% Analysis Date = 06/30/14 Pct Recovery = 61% Analysis Date = 06/30/14 Pct Recovery = 61% Analysis Date = 06/25/14 Pct Recovery = 61% Analysis Date = 06/25/14 Pct Recovery = 61% Analysis Date = 06/20/14 Pct Recovery = 61% Analysis Date = 06/20/14 Pct Recovery = 61% Analysis Date = 06/15/14 Pct Recovery = 61% Analysis Date = 06/15/14 Pct Recovery = 61% Analysis Date = 06/10/14 Pct Recovery = 61% Analysis Date = 06/10/14 Pct Recovery = 61% Analysis Date = 06/05/14 Pct Recovery = 61% Analysis Date = 06/05/14 Pct Recovery = 61% Analysis Date = 05/31/14 Pct Recovery = 60% Analysis Date = 05/31/14 Pct Recovery = 60% Analysis Date = 05/26/14 Pct Recovery = 60% Analysis Date = 05/26/14 Pct Recovery = 60% Analysis Date = 05/21/14 Pct Recovery = 60% Analysis Date = 05/21/14 Pct Recovery = 60% Analysis Date = 05/17/14 Pct Recovery = 60% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
PROPRANOLOL

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 1 49% . 49% 0%
>= Reporting Level 73 69% 10% 70% 10%
Total 74 69% 10% 70% 11%

Sample Statistics
PROPRANOLOL

Characteristic N % % Basis
Plotted 74 97% Spiked
Estimated Values 3 4% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 1 1% Spiked
Spiked 76 .  
False Negatives 1 1% 1 out of 76
Not Spiked 39 .  
False Positives 0 0% 0 out of 39

BQS OBSP Determination:
PSEUDOEPHEDRINE+EPHEDRINE
METHOD: 2440 , TESTIDCODE: 67460LCM56
Open Data Set

Analysis Date = 11/05/15 SpikeMix = ERA 0406-15-08: 80 µl & Abs 052215: 80 µl Pct Recovery = 85% Analysis Date = 11/04/15 SpikeMix = Abs 052215: 80 µl & Abs 050115: 80 µl Pct Recovery = 93% Analysis Date = 09/24/16 SpikeMix = Crescent EN160610015: 80 µl & Abs 061416: 80 µl Pct Recovery = 36% Analysis Date = 09/24/16 SpikeMix = Abs 061416: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 36% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 35% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 35% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 36% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 35% Analysis Date = 05/07/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 91% Analysis Date = 03/11/15 SpikeMix = ERA 0318-14-02: 15 µl & Abs 041714: 15 µl Pct Recovery = 80% Analysis Date = 01/16/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 86% Analysis Date = 12/06/14 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 72% Analysis Date = 08/21/14 SpikeMix = ERA 0318-14-02: 60 µl & Abs 041714: 60 µl Pct Recovery = 59% Analysis Date = 07/12/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 70% Analysis Date = 06/11/14 SpikeMix = Abs 041614: 60 µl & Abs 041714: 60 µl Pct Recovery = 76% Analysis Date = 05/21/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 72% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-08: 40 µl & Abs 052215: 40 µl Pct Recovery = 80% Analysis Date = 02/23/16 SpikeMix = Abs 052215: 40 µl & Abs 050115: 40 µl Pct Recovery = 84% Analysis Date = 09/10/15 SpikeMix = Abs 052215: 40 µl & ERA 0406-15-07A: 40 µl Pct Recovery = 84% Analysis Date = 07/31/15 SpikeMix = Abs 051315: 40 µl & Abs 052215: 40 µl Pct Recovery = 78% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 40% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 36% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 28% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 30% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 33% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 32% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 28% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 36% Analysis Date = 11/04/14 SpikeMix = Abs 041714: 8 µl & ERA 0319-14-05: 8 µl Pct Recovery = 63% Analysis Date = 10/10/14 SpikeMix = Abs 041714: 30 µl & Abs 041814: 30 µl Pct Recovery = 66% Analysis Date = 07/20/14 SpikeMix = ERA 0318-14-02: 30 µl & Abs 041714: 30 µl Pct Recovery = 65% Analysis Date = 06/28/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 74% Analysis Date = 05/17/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 76% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 82% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 74% Analysis Date = 02/23/16 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 69% Analysis Date = 11/24/15 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 84% Analysis Date = 09/09/15 SpikeMix = ERA 0406-15-08: 20 µl & Abs 052215: 20 µl Pct Recovery = 97% Analysis Date = 08/27/15 SpikeMix = Abs 052215: 20 µl & Abs 050115: 20 µl Pct Recovery = 76% Analysis Date = 07/09/15 SpikeMix = Abs 050115: 20 µl & Abs 052215: 20 µl Pct Recovery = 82% Analysis Date = 06/26/15 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 74% Analysis Date = 12/16/16 Pct Recovery = 21% Analysis Date = 12/11/16 Pct Recovery = 21% Analysis Date = 12/11/16 Pct Recovery = 21% Analysis Date = 12/06/16 Pct Recovery = 22% Analysis Date = 12/06/16 Pct Recovery = 22% Analysis Date = 12/01/16 Pct Recovery = 23% Analysis Date = 12/01/16 Pct Recovery = 23% Analysis Date = 11/27/16 Pct Recovery = 24% Analysis Date = 11/27/16 Pct Recovery = 24% Analysis Date = 11/22/16 Pct Recovery = 24% Analysis Date = 11/22/16 Pct Recovery = 24% Analysis Date = 11/17/16 Pct Recovery = 25% Analysis Date = 11/17/16 Pct Recovery = 25% Analysis Date = 11/12/16 Pct Recovery = 26% Analysis Date = 11/12/16 Pct Recovery = 26% Analysis Date = 11/08/16 Pct Recovery = 27% Analysis Date = 11/08/16 Pct Recovery = 27% Analysis Date = 11/03/16 Pct Recovery = 27% Analysis Date = 11/03/16 Pct Recovery = 27% Analysis Date = 10/29/16 Pct Recovery = 28% Analysis Date = 10/29/16 Pct Recovery = 28% Analysis Date = 10/25/16 Pct Recovery = 29% Analysis Date = 10/25/16 Pct Recovery = 29% Analysis Date = 10/20/16 Pct Recovery = 30% Analysis Date = 10/20/16 Pct Recovery = 30% Analysis Date = 10/15/16 Pct Recovery = 30% Analysis Date = 10/15/16 Pct Recovery = 30% Analysis Date = 10/10/16 Pct Recovery = 31% Analysis Date = 10/10/16 Pct Recovery = 31% Analysis Date = 10/06/16 Pct Recovery = 32% Analysis Date = 10/06/16 Pct Recovery = 32% Analysis Date = 10/01/16 Pct Recovery = 33% Analysis Date = 10/01/16 Pct Recovery = 33% Analysis Date = 09/26/16 Pct Recovery = 33% Analysis Date = 09/26/16 Pct Recovery = 33% Analysis Date = 09/22/16 Pct Recovery = 34% Analysis Date = 09/22/16 Pct Recovery = 34% Analysis Date = 09/17/16 Pct Recovery = 35% Analysis Date = 09/17/16 Pct Recovery = 35% Analysis Date = 09/12/16 Pct Recovery = 36% Analysis Date = 09/12/16 Pct Recovery = 36% Analysis Date = 09/07/16 Pct Recovery = 37% Analysis Date = 09/07/16 Pct Recovery = 37% Analysis Date = 09/03/16 Pct Recovery = 38% Analysis Date = 09/03/16 Pct Recovery = 38% Analysis Date = 08/29/16 Pct Recovery = 38% Analysis Date = 08/29/16 Pct Recovery = 38% Analysis Date = 08/24/16 Pct Recovery = 39% Analysis Date = 08/24/16 Pct Recovery = 39% Analysis Date = 08/20/16 Pct Recovery = 40% Analysis Date = 08/20/16 Pct Recovery = 40% Analysis Date = 08/15/16 Pct Recovery = 41% Analysis Date = 08/15/16 Pct Recovery = 41% Analysis Date = 08/10/16 Pct Recovery = 42% Analysis Date = 08/10/16 Pct Recovery = 42% Analysis Date = 08/05/16 Pct Recovery = 42% Analysis Date = 08/05/16 Pct Recovery = 42% Analysis Date = 08/01/16 Pct Recovery = 43% Analysis Date = 08/01/16 Pct Recovery = 43% Analysis Date = 07/27/16 Pct Recovery = 44% Analysis Date = 07/27/16 Pct Recovery = 44% Analysis Date = 07/22/16 Pct Recovery = 45% Analysis Date = 07/22/16 Pct Recovery = 45% Analysis Date = 07/17/16 Pct Recovery = 46% Analysis Date = 07/17/16 Pct Recovery = 46% Analysis Date = 07/13/16 Pct Recovery = 47% Analysis Date = 07/13/16 Pct Recovery = 47% Analysis Date = 07/08/16 Pct Recovery = 48% Analysis Date = 07/08/16 Pct Recovery = 48% Analysis Date = 07/03/16 Pct Recovery = 49% Analysis Date = 07/03/16 Pct Recovery = 49% Analysis Date = 06/29/16 Pct Recovery = 50% Analysis Date = 06/29/16 Pct Recovery = 50% Analysis Date = 06/24/16 Pct Recovery = 51% Analysis Date = 06/24/16 Pct Recovery = 51% Analysis Date = 06/19/16 Pct Recovery = 52% Analysis Date = 06/19/16 Pct Recovery = 52% Analysis Date = 06/14/16 Pct Recovery = 53% Analysis Date = 06/14/16 Pct Recovery = 53% Analysis Date = 06/10/16 Pct Recovery = 53% Analysis Date = 06/10/16 Pct Recovery = 53% Analysis Date = 06/05/16 Pct Recovery = 54% Analysis Date = 06/05/16 Pct Recovery = 54% Analysis Date = 05/31/16 Pct Recovery = 55% Analysis Date = 05/31/16 Pct Recovery = 55% Analysis Date = 05/27/16 Pct Recovery = 56% Analysis Date = 05/27/16 Pct Recovery = 56% Analysis Date = 05/22/16 Pct Recovery = 57% Analysis Date = 05/22/16 Pct Recovery = 57% Analysis Date = 05/17/16 Pct Recovery = 58% Analysis Date = 05/17/16 Pct Recovery = 58% Analysis Date = 05/12/16 Pct Recovery = 59% Analysis Date = 05/12/16 Pct Recovery = 59% Analysis Date = 05/08/16 Pct Recovery = 60% Analysis Date = 05/08/16 Pct Recovery = 60% Analysis Date = 05/03/16 Pct Recovery = 61% Analysis Date = 05/03/16 Pct Recovery = 61% Analysis Date = 04/28/16 Pct Recovery = 62% Analysis Date = 04/28/16 Pct Recovery = 62% Analysis Date = 04/24/16 Pct Recovery = 63% Analysis Date = 04/24/16 Pct Recovery = 63% Analysis Date = 04/19/16 Pct Recovery = 64% Analysis Date = 04/19/16 Pct Recovery = 64% Analysis Date = 04/14/16 Pct Recovery = 65% Analysis Date = 04/14/16 Pct Recovery = 65% Analysis Date = 04/09/16 Pct Recovery = 66% Analysis Date = 04/09/16 Pct Recovery = 66% Analysis Date = 04/05/16 Pct Recovery = 67% Analysis Date = 04/05/16 Pct Recovery = 67% Analysis Date = 03/31/16 Pct Recovery = 67% Analysis Date = 03/31/16 Pct Recovery = 67% Analysis Date = 03/26/16 Pct Recovery = 68% Analysis Date = 03/26/16 Pct Recovery = 68% Analysis Date = 03/21/16 Pct Recovery = 69% Analysis Date = 03/21/16 Pct Recovery = 69% Analysis Date = 03/17/16 Pct Recovery = 70% Analysis Date = 03/17/16 Pct Recovery = 70% Analysis Date = 03/12/16 Pct Recovery = 71% Analysis Date = 03/12/16 Pct Recovery = 71% Analysis Date = 03/07/16 Pct Recovery = 72% Analysis Date = 03/07/16 Pct Recovery = 72% Analysis Date = 03/03/16 Pct Recovery = 73% Analysis Date = 03/03/16 Pct Recovery = 73% Analysis Date = 02/27/16 Pct Recovery = 74% Analysis Date = 02/27/16 Pct Recovery = 74% Analysis Date = 02/22/16 Pct Recovery = 75% Analysis Date = 02/22/16 Pct Recovery = 75% Analysis Date = 02/17/16 Pct Recovery = 75% Analysis Date = 02/17/16 Pct Recovery = 75% Analysis Date = 02/13/16 Pct Recovery = 75% Analysis Date = 02/13/16 Pct Recovery = 75% Analysis Date = 02/08/16 Pct Recovery = 76% Analysis Date = 02/08/16 Pct Recovery = 76% Analysis Date = 02/03/16 Pct Recovery = 76% Analysis Date = 02/03/16 Pct Recovery = 76% Analysis Date = 01/30/16 Pct Recovery = 76% Analysis Date = 01/30/16 Pct Recovery = 76% Analysis Date = 01/25/16 Pct Recovery = 77% Analysis Date = 01/25/16 Pct Recovery = 77% Analysis Date = 01/20/16 Pct Recovery = 77% Analysis Date = 01/20/16 Pct Recovery = 77% Analysis Date = 01/15/16 Pct Recovery = 77% Analysis Date = 01/15/16 Pct Recovery = 77% Analysis Date = 01/11/16 Pct Recovery = 78% Analysis Date = 01/11/16 Pct Recovery = 78% Analysis Date = 01/06/16 Pct Recovery = 78% Analysis Date = 01/06/16 Pct Recovery = 78% Analysis Date = 01/01/16 Pct Recovery = 78% Analysis Date = 01/01/16 Pct Recovery = 78% Analysis Date = 12/28/15 Pct Recovery = 79% Analysis Date = 12/28/15 Pct Recovery = 79% Analysis Date = 12/23/15 Pct Recovery = 79% Analysis Date = 12/23/15 Pct Recovery = 79% Analysis Date = 12/18/15 Pct Recovery = 79% Analysis Date = 12/18/15 Pct Recovery = 79% Analysis Date = 12/13/15 Pct Recovery = 80% Analysis Date = 12/13/15 Pct Recovery = 80% Analysis Date = 12/09/15 Pct Recovery = 80% Analysis Date = 12/09/15 Pct Recovery = 80% Analysis Date = 12/04/15 Pct Recovery = 80% Analysis Date = 12/04/15 Pct Recovery = 80% Analysis Date = 11/29/15 Pct Recovery = 80% Analysis Date = 11/29/15 Pct Recovery = 80% Analysis Date = 11/24/15 Pct Recovery = 81% Analysis Date = 11/24/15 Pct Recovery = 81% Analysis Date = 11/20/15 Pct Recovery = 81% Analysis Date = 11/20/15 Pct Recovery = 81% Analysis Date = 11/15/15 Pct Recovery = 81% Analysis Date = 11/15/15 Pct Recovery = 81% Analysis Date = 11/10/15 Pct Recovery = 82% Analysis Date = 11/10/15 Pct Recovery = 82% Analysis Date = 11/06/15 Pct Recovery = 82% Analysis Date = 11/06/15 Pct Recovery = 82% Analysis Date = 11/01/15 Pct Recovery = 82% Analysis Date = 11/01/15 Pct Recovery = 82% Analysis Date = 10/27/15 Pct Recovery = 82% Analysis Date = 10/27/15 Pct Recovery = 82% Analysis Date = 10/22/15 Pct Recovery = 82% Analysis Date = 10/22/15 Pct Recovery = 82% Analysis Date = 10/18/15 Pct Recovery = 82% Analysis Date = 10/18/15 Pct Recovery = 82% Analysis Date = 10/13/15 Pct Recovery = 82% Analysis Date = 10/13/15 Pct Recovery = 82% Analysis Date = 10/08/15 Pct Recovery = 82% Analysis Date = 10/08/15 Pct Recovery = 82% Analysis Date = 10/04/15 Pct Recovery = 82% Analysis Date = 10/04/15 Pct Recovery = 82% Analysis Date = 09/29/15 Pct Recovery = 82% Analysis Date = 09/29/15 Pct Recovery = 82% Analysis Date = 09/24/15 Pct Recovery = 83% Analysis Date = 09/24/15 Pct Recovery = 83% Analysis Date = 09/19/15 Pct Recovery = 83% Analysis Date = 09/19/15 Pct Recovery = 83% Analysis Date = 09/15/15 Pct Recovery = 83% Analysis Date = 09/15/15 Pct Recovery = 83% Analysis Date = 09/10/15 Pct Recovery = 83% Analysis Date = 09/10/15 Pct Recovery = 83% Analysis Date = 09/05/15 Pct Recovery = 83% Analysis Date = 09/05/15 Pct Recovery = 83% Analysis Date = 09/01/15 Pct Recovery = 83% Analysis Date = 09/01/15 Pct Recovery = 83% Analysis Date = 08/27/15 Pct Recovery = 83% Analysis Date = 08/27/15 Pct Recovery = 83% Analysis Date = 08/22/15 Pct Recovery = 82% Analysis Date = 08/22/15 Pct Recovery = 82% Analysis Date = 08/17/15 Pct Recovery = 82% Analysis Date = 08/17/15 Pct Recovery = 82% Analysis Date = 08/13/15 Pct Recovery = 82% Analysis Date = 08/13/15 Pct Recovery = 82% Analysis Date = 08/08/15 Pct Recovery = 82% Analysis Date = 08/08/15 Pct Recovery = 82% Analysis Date = 08/03/15 Pct Recovery = 82% Analysis Date = 08/03/15 Pct Recovery = 82% Analysis Date = 07/29/15 Pct Recovery = 82% Analysis Date = 07/29/15 Pct Recovery = 82% Analysis Date = 07/25/15 Pct Recovery = 82% Analysis Date = 07/25/15 Pct Recovery = 82% Analysis Date = 07/20/15 Pct Recovery = 82% Analysis Date = 07/20/15 Pct Recovery = 82% Analysis Date = 07/15/15 Pct Recovery = 82% Analysis Date = 07/15/15 Pct Recovery = 82% Analysis Date = 07/11/15 Pct Recovery = 82% Analysis Date = 07/11/15 Pct Recovery = 82% Analysis Date = 07/06/15 Pct Recovery = 82% Analysis Date = 07/06/15 Pct Recovery = 82% Analysis Date = 07/01/15 Pct Recovery = 81% Analysis Date = 07/01/15 Pct Recovery = 81% Analysis Date = 06/26/15 Pct Recovery = 81% Analysis Date = 06/26/15 Pct Recovery = 81% Analysis Date = 06/22/15 Pct Recovery = 81% Analysis Date = 06/22/15 Pct Recovery = 81% Analysis Date = 06/17/15 Pct Recovery = 81% Analysis Date = 06/17/15 Pct Recovery = 81% Analysis Date = 06/12/15 Pct Recovery = 81% Analysis Date = 06/12/15 Pct Recovery = 81% Analysis Date = 06/08/15 Pct Recovery = 81% Analysis Date = 06/08/15 Pct Recovery = 81% Analysis Date = 06/03/15 Pct Recovery = 80% Analysis Date = 06/03/15 Pct Recovery = 80% Analysis Date = 05/29/15 Pct Recovery = 80% Analysis Date = 05/29/15 Pct Recovery = 80% Analysis Date = 05/24/15 Pct Recovery = 80% Analysis Date = 05/24/15 Pct Recovery = 80% Analysis Date = 05/20/15 Pct Recovery = 80% Analysis Date = 05/20/15 Pct Recovery = 80% Analysis Date = 05/15/15 Pct Recovery = 80% Analysis Date = 05/15/15 Pct Recovery = 80% Analysis Date = 05/10/15 Pct Recovery = 80% Analysis Date = 05/10/15 Pct Recovery = 80% Analysis Date = 05/06/15 Pct Recovery = 79% Analysis Date = 05/06/15 Pct Recovery = 79% Analysis Date = 05/01/15 Pct Recovery = 79% Analysis Date = 05/01/15 Pct Recovery = 79% Analysis Date = 04/26/15 Pct Recovery = 79% Analysis Date = 04/26/15 Pct Recovery = 79% Analysis Date = 04/21/15 Pct Recovery = 79% Analysis Date = 04/21/15 Pct Recovery = 79% Analysis Date = 04/17/15 Pct Recovery = 79% Analysis Date = 04/17/15 Pct Recovery = 79% Analysis Date = 04/12/15 Pct Recovery = 79% Analysis Date = 04/12/15 Pct Recovery = 79% Analysis Date = 04/07/15 Pct Recovery = 79% Analysis Date = 04/07/15 Pct Recovery = 79% Analysis Date = 04/02/15 Pct Recovery = 78% Analysis Date = 04/02/15 Pct Recovery = 78% Analysis Date = 03/29/15 Pct Recovery = 78% Analysis Date = 03/29/15 Pct Recovery = 78% Analysis Date = 03/24/15 Pct Recovery = 78% Analysis Date = 03/24/15 Pct Recovery = 78% Analysis Date = 03/19/15 Pct Recovery = 78% Analysis Date = 03/19/15 Pct Recovery = 78% Analysis Date = 03/15/15 Pct Recovery = 78% Analysis Date = 03/15/15 Pct Recovery = 78% Analysis Date = 03/10/15 Pct Recovery = 78% Analysis Date = 03/10/15 Pct Recovery = 78% Analysis Date = 03/05/15 Pct Recovery = 77% Analysis Date = 03/05/15 Pct Recovery = 77% Analysis Date = 02/28/15 Pct Recovery = 77% Analysis Date = 02/28/15 Pct Recovery = 77% Analysis Date = 02/24/15 Pct Recovery = 77% Analysis Date = 02/24/15 Pct Recovery = 77% Analysis Date = 02/19/15 Pct Recovery = 77% Analysis Date = 02/19/15 Pct Recovery = 77% Analysis Date = 02/14/15 Pct Recovery = 77% Analysis Date = 02/14/15 Pct Recovery = 77% Analysis Date = 02/10/15 Pct Recovery = 77% Analysis Date = 02/10/15 Pct Recovery = 77% Analysis Date = 02/05/15 Pct Recovery = 76% Analysis Date = 02/05/15 Pct Recovery = 76% Analysis Date = 01/31/15 Pct Recovery = 76% Analysis Date = 01/31/15 Pct Recovery = 76% Analysis Date = 01/26/15 Pct Recovery = 76% Analysis Date = 01/26/15 Pct Recovery = 76% Analysis Date = 01/22/15 Pct Recovery = 76% Analysis Date = 01/22/15 Pct Recovery = 76% Analysis Date = 01/17/15 Pct Recovery = 76% Analysis Date = 01/17/15 Pct Recovery = 76% Analysis Date = 01/12/15 Pct Recovery = 76% Analysis Date = 01/12/15 Pct Recovery = 76% Analysis Date = 01/08/15 Pct Recovery = 75% Analysis Date = 01/08/15 Pct Recovery = 75% Analysis Date = 01/03/15 Pct Recovery = 75% Analysis Date = 01/03/15 Pct Recovery = 75% Analysis Date = 12/29/14 Pct Recovery = 75% Analysis Date = 12/29/14 Pct Recovery = 75% Analysis Date = 12/24/14 Pct Recovery = 75% Analysis Date = 12/24/14 Pct Recovery = 75% Analysis Date = 12/20/14 Pct Recovery = 75% Analysis Date = 12/20/14 Pct Recovery = 75% Analysis Date = 12/15/14 Pct Recovery = 75% Analysis Date = 12/15/14 Pct Recovery = 75% Analysis Date = 12/10/14 Pct Recovery = 75% Analysis Date = 12/10/14 Pct Recovery = 75% Analysis Date = 12/05/14 Pct Recovery = 75% Analysis Date = 12/05/14 Pct Recovery = 75% Analysis Date = 12/01/14 Pct Recovery = 74% Analysis Date = 12/01/14 Pct Recovery = 74% Analysis Date = 11/26/14 Pct Recovery = 74% Analysis Date = 11/26/14 Pct Recovery = 74% Analysis Date = 11/21/14 Pct Recovery = 74% Analysis Date = 11/21/14 Pct Recovery = 74% Analysis Date = 11/17/14 Pct Recovery = 74% Analysis Date = 11/17/14 Pct Recovery = 74% Analysis Date = 11/12/14 Pct Recovery = 74% Analysis Date = 11/12/14 Pct Recovery = 74% Analysis Date = 11/07/14 Pct Recovery = 74% Analysis Date = 11/07/14 Pct Recovery = 74% Analysis Date = 11/02/14 Pct Recovery = 74% Analysis Date = 11/02/14 Pct Recovery = 74% Analysis Date = 10/29/14 Pct Recovery = 73% Analysis Date = 10/29/14 Pct Recovery = 73% Analysis Date = 10/24/14 Pct Recovery = 73% Analysis Date = 10/24/14 Pct Recovery = 73% Analysis Date = 10/19/14 Pct Recovery = 73% Analysis Date = 10/19/14 Pct Recovery = 73% Analysis Date = 10/15/14 Pct Recovery = 73% Analysis Date = 10/15/14 Pct Recovery = 73% Analysis Date = 10/10/14 Pct Recovery = 73% Analysis Date = 10/10/14 Pct Recovery = 73% Analysis Date = 10/05/14 Pct Recovery = 73% Analysis Date = 10/05/14 Pct Recovery = 73% Analysis Date = 09/30/14 Pct Recovery = 73% Analysis Date = 09/30/14 Pct Recovery = 73% Analysis Date = 09/26/14 Pct Recovery = 72% Analysis Date = 09/26/14 Pct Recovery = 72% Analysis Date = 09/21/14 Pct Recovery = 72% Analysis Date = 09/21/14 Pct Recovery = 72% Analysis Date = 09/16/14 Pct Recovery = 72% Analysis Date = 09/16/14 Pct Recovery = 72% Analysis Date = 09/12/14 Pct Recovery = 72% Analysis Date = 09/12/14 Pct Recovery = 72% Analysis Date = 09/07/14 Pct Recovery = 72% Analysis Date = 09/07/14 Pct Recovery = 72% Analysis Date = 09/02/14 Pct Recovery = 72% Analysis Date = 09/02/14 Pct Recovery = 72% Analysis Date = 08/28/14 Pct Recovery = 72% Analysis Date = 08/28/14 Pct Recovery = 72% Analysis Date = 08/24/14 Pct Recovery = 71% Analysis Date = 08/24/14 Pct Recovery = 71% Analysis Date = 08/19/14 Pct Recovery = 71% Analysis Date = 08/19/14 Pct Recovery = 71% Analysis Date = 08/14/14 Pct Recovery = 71% Analysis Date = 08/14/14 Pct Recovery = 71% Analysis Date = 08/09/14 Pct Recovery = 71% Analysis Date = 08/09/14 Pct Recovery = 71% Analysis Date = 08/05/14 Pct Recovery = 71% Analysis Date = 08/05/14 Pct Recovery = 71% Analysis Date = 07/31/14 Pct Recovery = 71% Analysis Date = 07/31/14 Pct Recovery = 71% Analysis Date = 07/26/14 Pct Recovery = 71% Analysis Date = 07/26/14 Pct Recovery = 71% Analysis Date = 07/22/14 Pct Recovery = 70% Analysis Date = 07/22/14 Pct Recovery = 70% Analysis Date = 07/17/14 Pct Recovery = 70% Analysis Date = 07/17/14 Pct Recovery = 70% Analysis Date = 07/12/14 Pct Recovery = 70% Analysis Date = 07/12/14 Pct Recovery = 70% Analysis Date = 07/07/14 Pct Recovery = 70% Analysis Date = 07/07/14 Pct Recovery = 70% Analysis Date = 07/03/14 Pct Recovery = 70% Analysis Date = 07/03/14 Pct Recovery = 70% Analysis Date = 06/28/14 Pct Recovery = 70% Analysis Date = 06/28/14 Pct Recovery = 70% Analysis Date = 06/23/14 Pct Recovery = 70% Analysis Date = 06/23/14 Pct Recovery = 70% Analysis Date = 06/19/14 Pct Recovery = 69% Analysis Date = 06/19/14 Pct Recovery = 69% Analysis Date = 06/14/14 Pct Recovery = 69% Analysis Date = 06/14/14 Pct Recovery = 69% Analysis Date = 06/09/14 Pct Recovery = 69% Analysis Date = 06/09/14 Pct Recovery = 69% Analysis Date = 06/04/14 Pct Recovery = 69% Analysis Date = 06/04/14 Pct Recovery = 69% Analysis Date = 05/31/14 Pct Recovery = 69% Analysis Date = 05/31/14 Pct Recovery = 69% Analysis Date = 05/26/14 Pct Recovery = 69% Analysis Date = 05/26/14 Pct Recovery = 69% Analysis Date = 05/21/14 Pct Recovery = 69% Analysis Date = 05/21/14 Pct Recovery = 69% Analysis Date = 05/17/14 Pct Recovery = 69% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
PSEUDOEPHEDRINE+EPHEDRINE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 41 63% 22% 72% 33%
Total 41 63% 22% 72% 33%

Sample Statistics
PSEUDOEPHEDRINE+EPHEDRINE

Characteristic N % % Basis
Plotted 41 100% Spiked
Estimated Values 3 7% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 41 .  
False Negatives 0 0% 0 out of 41
Not Spiked 74 .  
False Positives 0 0% 0 out of 74

BQS OBSP Determination:
QUININE
METHOD: 2440 , TESTIDCODE: 68011LCM56
Open Data Set

Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 64% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 63% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 64% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 63% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 80 µl & ERA 0406-15-08: 80 µl Pct Recovery = 65% Analysis Date = 11/04/15 SpikeMix = Abs 052215: 80 µl & Abs 050115: 80 µl Pct Recovery = 69% Analysis Date = 01/17/16 SpikeMix = ERA 0406-15-09: 80 µl & ERA 0406-15-07A: 80 µl Pct Recovery = 71% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 80 µl & Abs 051315: 80 µl Pct Recovery = 134% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 48% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 54% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 55% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 49% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 60% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 45% Analysis Date = 09/24/16 SpikeMix = Crescent EN160610015: 80 µl & Abs 061416: 80 µl Pct Recovery = 81% Analysis Date = 09/24/16 SpikeMix = Abs 061416: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 72% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 68% Analysis Date = 12/07/14 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 49% Analysis Date = 10/25/14 SpikeMix = Abs 041614: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 61% Analysis Date = 06/22/14 SpikeMix = Abs 041814: 60 µl & Abs 041614: 60 µl Pct Recovery = 81% Analysis Date = 06/11/14 SpikeMix = Abs 041614: 60 µl & Abs 041714: 60 µl Pct Recovery = 59% Analysis Date = 04/29/15 SpikeMix = ERA 0319-14-05: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 89% Analysis Date = 03/11/15 SpikeMix = ERA 0318-14-02: 15 µl & Abs 041714: 15 µl Pct Recovery = 91% Analysis Date = 02/06/15 SpikeMix = Abs 041814: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 60% Analysis Date = 12/06/14 SpikeMix = ERA 0318-14-02: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 48% Analysis Date = 10/11/14 SpikeMix = ERA 0318-14-02: 60 µl & ERA 0319-14-04: 60 µl Pct Recovery = 81% Analysis Date = 08/21/14 SpikeMix = ERA 0318-14-02: 60 µl & Abs 041714: 60 µl Pct Recovery = 53% Analysis Date = 07/26/14 SpikeMix = ERA 0319-14-05: 60 µl & ERA 0318-14-02: 60 µl Pct Recovery = 76% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 90% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 85% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 35% Analysis Date = 02/23/16 SpikeMix = Abs 052215: 40 µl & Abs 050115: 40 µl Pct Recovery = 71% Analysis Date = 07/31/15 SpikeMix = ERA 0406-15-09: 40 µl & Abs 050115: 40 µl Pct Recovery = 78% Analysis Date = 07/30/15 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 61% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-07A: 40 µl & Abs 051315: 40 µl Pct Recovery = 68% Analysis Date = 11/04/15 SpikeMix = ERA 0406-15-07A: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 73% Analysis Date = 09/10/15 SpikeMix = Abs 052215: 40 µl & ERA 0406-15-07A: 40 µl Pct Recovery = 78% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 42% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 41% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 56% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 59% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 46% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 56% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 52% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 46% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 55% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 62% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 72% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 96% Analysis Date = 04/30/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 66% Analysis Date = 02/10/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 33% Analysis Date = 10/24/14 SpikeMix = ERA 0319-14-05: 8 µl & Abs 041614: 8 µl Pct Recovery = 57% Analysis Date = 12/07/14 SpikeMix = ERA 0318-14-02: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 70% Analysis Date = 11/04/14 SpikeMix = Abs 041814: 8 µl & ERA 0318-14-02: 8 µl Pct Recovery = 34% Analysis Date = 04/23/14 SpikeMix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.2: 20 µl Pct Recovery = 75% Analysis Date = 09/12/14 SpikeMix = Abs 041614: 30 µl & ERA 0319-14-04: 30 µl Pct Recovery = 51% Analysis Date = 07/13/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 73% Analysis Date = 06/28/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 63% Analysis Date = 05/30/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 63% Analysis Date = 05/17/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 58% Analysis Date = 10/10/14 SpikeMix = Abs 041814: 30 µl & ERA 0318-14-02: 30 µl Pct Recovery = 72% Analysis Date = 08/30/14 SpikeMix = ERA 0318-14-02: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 62% Analysis Date = 07/20/14 SpikeMix = ERA 0318-14-02: 30 µl & Abs 041714: 30 µl Pct Recovery = 52% Analysis Date = 11/25/15 SpikeMix = Abs 050115: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 83% Analysis Date = 11/24/15 SpikeMix = ERA 0406-15-09: 20 µl & Abs 050115: 20 µl Pct Recovery = 88% Analysis Date = 08/27/15 SpikeMix = Abs 052215: 20 µl & Abs 050115: 20 µl Pct Recovery = 53% Analysis Date = 08/11/15 SpikeMix = Abs 050115: 20 µl & Abs 051315: 20 µl Pct Recovery = 41% Analysis Date = 07/09/15 SpikeMix = Abs 050115: 20 µl & Abs 052215: 20 µl Pct Recovery = 77% Analysis Date = 06/09/15 SpikeMix = Abs 051315: 20 µl & Abs 050115: 20 µl Pct Recovery = 48% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 67% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 60% Analysis Date = 04/27/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 98% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 78% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 69% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 72% Analysis Date = 11/24/15 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 83% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-09: 20 µl Pct Recovery = 118% Analysis Date = 01/18/17 Pct Recovery = 55% Analysis Date = 01/13/17 Pct Recovery = 55% Analysis Date = 01/13/17 Pct Recovery = 55% Analysis Date = 01/08/17 Pct Recovery = 56% Analysis Date = 01/08/17 Pct Recovery = 56% Analysis Date = 01/03/17 Pct Recovery = 56% Analysis Date = 01/03/17 Pct Recovery = 56% Analysis Date = 12/29/16 Pct Recovery = 56% Analysis Date = 12/29/16 Pct Recovery = 56% Analysis Date = 12/24/16 Pct Recovery = 56% Analysis Date = 12/24/16 Pct Recovery = 56% Analysis Date = 12/19/16 Pct Recovery = 56% Analysis Date = 12/19/16 Pct Recovery = 56% Analysis Date = 12/14/16 Pct Recovery = 57% Analysis Date = 12/14/16 Pct Recovery = 57% Analysis Date = 12/09/16 Pct Recovery = 57% Analysis Date = 12/09/16 Pct Recovery = 57% Analysis Date = 12/04/16 Pct Recovery = 57% Analysis Date = 12/04/16 Pct Recovery = 57% Analysis Date = 11/29/16 Pct Recovery = 57% Analysis Date = 11/29/16 Pct Recovery = 57% Analysis Date = 11/24/16 Pct Recovery = 58% Analysis Date = 11/24/16 Pct Recovery = 58% Analysis Date = 11/19/16 Pct Recovery = 58% Analysis Date = 11/19/16 Pct Recovery = 58% Analysis Date = 11/14/16 Pct Recovery = 58% Analysis Date = 11/14/16 Pct Recovery = 58% Analysis Date = 11/09/16 Pct Recovery = 58% Analysis Date = 11/09/16 Pct Recovery = 58% Analysis Date = 11/04/16 Pct Recovery = 59% Analysis Date = 11/04/16 Pct Recovery = 59% Analysis Date = 10/30/16 Pct Recovery = 59% Analysis Date = 10/30/16 Pct Recovery = 59% Analysis Date = 10/25/16 Pct Recovery = 59% Analysis Date = 10/25/16 Pct Recovery = 59% Analysis Date = 10/20/16 Pct Recovery = 59% Analysis Date = 10/20/16 Pct Recovery = 59% Analysis Date = 10/15/16 Pct Recovery = 59% Analysis Date = 10/15/16 Pct Recovery = 59% Analysis Date = 10/10/16 Pct Recovery = 60% Analysis Date = 10/10/16 Pct Recovery = 60% Analysis Date = 10/05/16 Pct Recovery = 60% Analysis Date = 10/05/16 Pct Recovery = 60% Analysis Date = 09/30/16 Pct Recovery = 60% Analysis Date = 09/30/16 Pct Recovery = 60% Analysis Date = 09/25/16 Pct Recovery = 60% Analysis Date = 09/25/16 Pct Recovery = 60% Analysis Date = 09/20/16 Pct Recovery = 61% Analysis Date = 09/20/16 Pct Recovery = 61% Analysis Date = 09/15/16 Pct Recovery = 61% Analysis Date = 09/15/16 Pct Recovery = 61% Analysis Date = 09/10/16 Pct Recovery = 61% Analysis Date = 09/10/16 Pct Recovery = 61% Analysis Date = 09/05/16 Pct Recovery = 61% Analysis Date = 09/05/16 Pct Recovery = 61% Analysis Date = 08/31/16 Pct Recovery = 62% Analysis Date = 08/31/16 Pct Recovery = 62% Analysis Date = 08/26/16 Pct Recovery = 62% Analysis Date = 08/26/16 Pct Recovery = 62% Analysis Date = 08/21/16 Pct Recovery = 62% Analysis Date = 08/21/16 Pct Recovery = 62% Analysis Date = 08/16/16 Pct Recovery = 62% Analysis Date = 08/16/16 Pct Recovery = 62% Analysis Date = 08/11/16 Pct Recovery = 63% Analysis Date = 08/11/16 Pct Recovery = 63% Analysis Date = 08/06/16 Pct Recovery = 63% Analysis Date = 08/06/16 Pct Recovery = 63% Analysis Date = 08/01/16 Pct Recovery = 63% Analysis Date = 08/01/16 Pct Recovery = 63% Analysis Date = 07/27/16 Pct Recovery = 63% Analysis Date = 07/27/16 Pct Recovery = 63% Analysis Date = 07/22/16 Pct Recovery = 64% Analysis Date = 07/22/16 Pct Recovery = 64% Analysis Date = 07/17/16 Pct Recovery = 64% Analysis Date = 07/17/16 Pct Recovery = 64% Analysis Date = 07/12/16 Pct Recovery = 64% Analysis Date = 07/12/16 Pct Recovery = 64% Analysis Date = 07/07/16 Pct Recovery = 65% Analysis Date = 07/07/16 Pct Recovery = 65% Analysis Date = 07/02/16 Pct Recovery = 65% Analysis Date = 07/02/16 Pct Recovery = 65% Analysis Date = 06/27/16 Pct Recovery = 65% Analysis Date = 06/27/16 Pct Recovery = 65% Analysis Date = 06/22/16 Pct Recovery = 65% Analysis Date = 06/22/16 Pct Recovery = 65% Analysis Date = 06/17/16 Pct Recovery = 66% Analysis Date = 06/17/16 Pct Recovery = 66% Analysis Date = 06/12/16 Pct Recovery = 66% Analysis Date = 06/12/16 Pct Recovery = 66% Analysis Date = 06/07/16 Pct Recovery = 66% Analysis Date = 06/07/16 Pct Recovery = 66% Analysis Date = 06/02/16 Pct Recovery = 66% Analysis Date = 06/02/16 Pct Recovery = 66% Analysis Date = 05/28/16 Pct Recovery = 67% Analysis Date = 05/28/16 Pct Recovery = 67% Analysis Date = 05/23/16 Pct Recovery = 67% Analysis Date = 05/23/16 Pct Recovery = 67% Analysis Date = 05/18/16 Pct Recovery = 67% Analysis Date = 05/18/16 Pct Recovery = 67% Analysis Date = 05/13/16 Pct Recovery = 68% Analysis Date = 05/13/16 Pct Recovery = 68% Analysis Date = 05/08/16 Pct Recovery = 68% Analysis Date = 05/08/16 Pct Recovery = 68% Analysis Date = 05/03/16 Pct Recovery = 68% Analysis Date = 05/03/16 Pct Recovery = 68% Analysis Date = 04/28/16 Pct Recovery = 68% Analysis Date = 04/28/16 Pct Recovery = 68% Analysis Date = 04/23/16 Pct Recovery = 69% Analysis Date = 04/23/16 Pct Recovery = 69% Analysis Date = 04/18/16 Pct Recovery = 69% Analysis Date = 04/18/16 Pct Recovery = 69% Analysis Date = 04/13/16 Pct Recovery = 69% Analysis Date = 04/13/16 Pct Recovery = 69% Analysis Date = 04/08/16 Pct Recovery = 70% Analysis Date = 04/08/16 Pct Recovery = 70% Analysis Date = 04/03/16 Pct Recovery = 70% Analysis Date = 04/03/16 Pct Recovery = 70% Analysis Date = 03/29/16 Pct Recovery = 70% Analysis Date = 03/29/16 Pct Recovery = 70% Analysis Date = 03/24/16 Pct Recovery = 71% Analysis Date = 03/24/16 Pct Recovery = 71% Analysis Date = 03/19/16 Pct Recovery = 71% Analysis Date = 03/19/16 Pct Recovery = 71% Analysis Date = 03/14/16 Pct Recovery = 72% Analysis Date = 03/14/16 Pct Recovery = 72% Analysis Date = 03/09/16 Pct Recovery = 72% Analysis Date = 03/09/16 Pct Recovery = 72% Analysis Date = 03/04/16 Pct Recovery = 72% Analysis Date = 03/04/16 Pct Recovery = 72% Analysis Date = 02/28/16 Pct Recovery = 73% Analysis Date = 02/28/16 Pct Recovery = 73% Analysis Date = 02/23/16 Pct Recovery = 73% Analysis Date = 02/23/16 Pct Recovery = 73% Analysis Date = 02/18/16 Pct Recovery = 73% Analysis Date = 02/18/16 Pct Recovery = 73% Analysis Date = 02/13/16 Pct Recovery = 73% Analysis Date = 02/13/16 Pct Recovery = 73% Analysis Date = 02/08/16 Pct Recovery = 73% Analysis Date = 02/08/16 Pct Recovery = 73% Analysis Date = 02/03/16 Pct Recovery = 73% Analysis Date = 02/03/16 Pct Recovery = 73% Analysis Date = 01/29/16 Pct Recovery = 73% Analysis Date = 01/29/16 Pct Recovery = 73% Analysis Date = 01/24/16 Pct Recovery = 74% Analysis Date = 01/24/16 Pct Recovery = 74% Analysis Date = 01/19/16 Pct Recovery = 74% Analysis Date = 01/19/16 Pct Recovery = 74% Analysis Date = 01/14/16 Pct Recovery = 74% Analysis Date = 01/14/16 Pct Recovery = 74% Analysis Date = 01/09/16 Pct Recovery = 74% Analysis Date = 01/09/16 Pct Recovery = 74% Analysis Date = 01/04/16 Pct Recovery = 74% Analysis Date = 01/04/16 Pct Recovery = 74% Analysis Date = 12/30/15 Pct Recovery = 74% Analysis Date = 12/30/15 Pct Recovery = 74% Analysis Date = 12/25/15 Pct Recovery = 74% Analysis Date = 12/25/15 Pct Recovery = 74% Analysis Date = 12/20/15 Pct Recovery = 74% Analysis Date = 12/20/15 Pct Recovery = 74% Analysis Date = 12/15/15 Pct Recovery = 74% Analysis Date = 12/15/15 Pct Recovery = 74% Analysis Date = 12/10/15 Pct Recovery = 75% Analysis Date = 12/10/15 Pct Recovery = 75% Analysis Date = 12/05/15 Pct Recovery = 75% Analysis Date = 12/05/15 Pct Recovery = 75% Analysis Date = 11/30/15 Pct Recovery = 75% Analysis Date = 11/30/15 Pct Recovery = 75% Analysis Date = 11/25/15 Pct Recovery = 75% Analysis Date = 11/25/15 Pct Recovery = 75% Analysis Date = 11/20/15 Pct Recovery = 75% Analysis Date = 11/20/15 Pct Recovery = 75% Analysis Date = 11/15/15 Pct Recovery = 75% Analysis Date = 11/15/15 Pct Recovery = 75% Analysis Date = 11/10/15 Pct Recovery = 75% Analysis Date = 11/10/15 Pct Recovery = 75% Analysis Date = 11/05/15 Pct Recovery = 74% Analysis Date = 11/05/15 Pct Recovery = 74% Analysis Date = 10/31/15 Pct Recovery = 74% Analysis Date = 10/31/15 Pct Recovery = 74% Analysis Date = 10/26/15 Pct Recovery = 74% Analysis Date = 10/26/15 Pct Recovery = 74% Analysis Date = 10/21/15 Pct Recovery = 74% Analysis Date = 10/21/15 Pct Recovery = 74% Analysis Date = 10/16/15 Pct Recovery = 74% Analysis Date = 10/16/15 Pct Recovery = 74% Analysis Date = 10/11/15 Pct Recovery = 74% Analysis Date = 10/11/15 Pct Recovery = 74% Analysis Date = 10/06/15 Pct Recovery = 74% Analysis Date = 10/06/15 Pct Recovery = 74% Analysis Date = 10/01/15 Pct Recovery = 73% Analysis Date = 10/01/15 Pct Recovery = 73% Analysis Date = 09/26/15 Pct Recovery = 73% Analysis Date = 09/26/15 Pct Recovery = 73% Analysis Date = 09/21/15 Pct Recovery = 73% Analysis Date = 09/21/15 Pct Recovery = 73% Analysis Date = 09/16/15 Pct Recovery = 73% Analysis Date = 09/16/15 Pct Recovery = 73% Analysis Date = 09/11/15 Pct Recovery = 73% Analysis Date = 09/11/15 Pct Recovery = 73% Analysis Date = 09/05/15 Pct Recovery = 73% Analysis Date = 09/05/15 Pct Recovery = 73% Analysis Date = 08/31/15 Pct Recovery = 73% Analysis Date = 08/31/15 Pct Recovery = 73% Analysis Date = 08/26/15 Pct Recovery = 72% Analysis Date = 08/26/15 Pct Recovery = 72% Analysis Date = 08/21/15 Pct Recovery = 72% Analysis Date = 08/21/15 Pct Recovery = 72% Analysis Date = 08/16/15 Pct Recovery = 72% Analysis Date = 08/16/15 Pct Recovery = 72% Analysis Date = 08/11/15 Pct Recovery = 72% Analysis Date = 08/11/15 Pct Recovery = 72% Analysis Date = 08/06/15 Pct Recovery = 72% Analysis Date = 08/06/15 Pct Recovery = 72% Analysis Date = 08/01/15 Pct Recovery = 72% Analysis Date = 08/01/15 Pct Recovery = 72% Analysis Date = 07/27/15 Pct Recovery = 72% Analysis Date = 07/27/15 Pct Recovery = 72% Analysis Date = 07/22/15 Pct Recovery = 71% Analysis Date = 07/22/15 Pct Recovery = 71% Analysis Date = 07/17/15 Pct Recovery = 71% Analysis Date = 07/17/15 Pct Recovery = 71% Analysis Date = 07/12/15 Pct Recovery = 71% Analysis Date = 07/12/15 Pct Recovery = 71% Analysis Date = 07/07/15 Pct Recovery = 71% Analysis Date = 07/07/15 Pct Recovery = 71% Analysis Date = 07/02/15 Pct Recovery = 71% Analysis Date = 07/02/15 Pct Recovery = 71% Analysis Date = 06/27/15 Pct Recovery = 70% Analysis Date = 06/27/15 Pct Recovery = 70% Analysis Date = 06/22/15 Pct Recovery = 70% Analysis Date = 06/22/15 Pct Recovery = 70% Analysis Date = 06/17/15 Pct Recovery = 70% Analysis Date = 06/17/15 Pct Recovery = 70% Analysis Date = 06/12/15 Pct Recovery = 70% Analysis Date = 06/12/15 Pct Recovery = 70% Analysis Date = 06/07/15 Pct Recovery = 70% Analysis Date = 06/07/15 Pct Recovery = 70% Analysis Date = 06/02/15 Pct Recovery = 70% Analysis Date = 06/02/15 Pct Recovery = 70% Analysis Date = 05/28/15 Pct Recovery = 69% Analysis Date = 05/28/15 Pct Recovery = 69% Analysis Date = 05/23/15 Pct Recovery = 69% Analysis Date = 05/23/15 Pct Recovery = 69% Analysis Date = 05/18/15 Pct Recovery = 69% Analysis Date = 05/18/15 Pct Recovery = 69% Analysis Date = 05/13/15 Pct Recovery = 69% Analysis Date = 05/13/15 Pct Recovery = 69% Analysis Date = 05/08/15 Pct Recovery = 69% Analysis Date = 05/08/15 Pct Recovery = 69% Analysis Date = 05/03/15 Pct Recovery = 68% Analysis Date = 05/03/15 Pct Recovery = 68% Analysis Date = 04/28/15 Pct Recovery = 68% Analysis Date = 04/28/15 Pct Recovery = 68% Analysis Date = 04/23/15 Pct Recovery = 68% Analysis Date = 04/23/15 Pct Recovery = 68% Analysis Date = 04/18/15 Pct Recovery = 68% Analysis Date = 04/18/15 Pct Recovery = 68% Analysis Date = 04/13/15 Pct Recovery = 68% Analysis Date = 04/13/15 Pct Recovery = 68% Analysis Date = 04/08/15 Pct Recovery = 68% Analysis Date = 04/08/15 Pct Recovery = 68% Analysis Date = 04/03/15 Pct Recovery = 68% Analysis Date = 04/03/15 Pct Recovery = 68% Analysis Date = 03/29/15 Pct Recovery = 67% Analysis Date = 03/29/15 Pct Recovery = 67% Analysis Date = 03/24/15 Pct Recovery = 67% Analysis Date = 03/24/15 Pct Recovery = 67% Analysis Date = 03/19/15 Pct Recovery = 67% Analysis Date = 03/19/15 Pct Recovery = 67% Analysis Date = 03/14/15 Pct Recovery = 67% Analysis Date = 03/14/15 Pct Recovery = 67% Analysis Date = 03/09/15 Pct Recovery = 67% Analysis Date = 03/09/15 Pct Recovery = 67% Analysis Date = 03/04/15 Pct Recovery = 67% Analysis Date = 03/04/15 Pct Recovery = 67% Analysis Date = 02/27/15 Pct Recovery = 67% Analysis Date = 02/27/15 Pct Recovery = 67% Analysis Date = 02/22/15 Pct Recovery = 66% Analysis Date = 02/22/15 Pct Recovery = 66% Analysis Date = 02/17/15 Pct Recovery = 66% Analysis Date = 02/17/15 Pct Recovery = 66% Analysis Date = 02/12/15 Pct Recovery = 66% Analysis Date = 02/12/15 Pct Recovery = 66% Analysis Date = 02/07/15 Pct Recovery = 66% Analysis Date = 02/07/15 Pct Recovery = 66% Analysis Date = 02/02/15 Pct Recovery = 66% Analysis Date = 02/02/15 Pct Recovery = 66% Analysis Date = 01/28/15 Pct Recovery = 66% Analysis Date = 01/28/15 Pct Recovery = 66% Analysis Date = 01/23/15 Pct Recovery = 66% Analysis Date = 01/23/15 Pct Recovery = 66% Analysis Date = 01/18/15 Pct Recovery = 66% Analysis Date = 01/18/15 Pct Recovery = 66% Analysis Date = 01/13/15 Pct Recovery = 65% Analysis Date = 01/13/15 Pct Recovery = 65% Analysis Date = 01/08/15 Pct Recovery = 65% Analysis Date = 01/08/15 Pct Recovery = 65% Analysis Date = 01/03/15 Pct Recovery = 65% Analysis Date = 01/03/15 Pct Recovery = 65% Analysis Date = 12/29/14 Pct Recovery = 65% Analysis Date = 12/29/14 Pct Recovery = 65% Analysis Date = 12/24/14 Pct Recovery = 65% Analysis Date = 12/24/14 Pct Recovery = 65% Analysis Date = 12/19/14 Pct Recovery = 65% Analysis Date = 12/19/14 Pct Recovery = 65% Analysis Date = 12/14/14 Pct Recovery = 65% Analysis Date = 12/14/14 Pct Recovery = 65% Analysis Date = 12/09/14 Pct Recovery = 64% Analysis Date = 12/09/14 Pct Recovery = 64% Analysis Date = 12/04/14 Pct Recovery = 64% Analysis Date = 12/04/14 Pct Recovery = 64% Analysis Date = 11/29/14 Pct Recovery = 64% Analysis Date = 11/29/14 Pct Recovery = 64% Analysis Date = 11/24/14 Pct Recovery = 64% Analysis Date = 11/24/14 Pct Recovery = 64% Analysis Date = 11/19/14 Pct Recovery = 64% Analysis Date = 11/19/14 Pct Recovery = 64% Analysis Date = 11/14/14 Pct Recovery = 64% Analysis Date = 11/14/14 Pct Recovery = 64% Analysis Date = 11/09/14 Pct Recovery = 64% Analysis Date = 11/09/14 Pct Recovery = 64% Analysis Date = 11/04/14 Pct Recovery = 64% Analysis Date = 11/04/14 Pct Recovery = 64% Analysis Date = 10/30/14 Pct Recovery = 64% Analysis Date = 10/30/14 Pct Recovery = 64% Analysis Date = 10/25/14 Pct Recovery = 64% Analysis Date = 10/25/14 Pct Recovery = 64% Analysis Date = 10/20/14 Pct Recovery = 63% Analysis Date = 10/20/14 Pct Recovery = 63% Analysis Date = 10/15/14 Pct Recovery = 63% Analysis Date = 10/15/14 Pct Recovery = 63% Analysis Date = 10/10/14 Pct Recovery = 63% Analysis Date = 10/10/14 Pct Recovery = 63% Analysis Date = 10/05/14 Pct Recovery = 63% Analysis Date = 10/05/14 Pct Recovery = 63% Analysis Date = 09/30/14 Pct Recovery = 63% Analysis Date = 09/30/14 Pct Recovery = 63% Analysis Date = 09/25/14 Pct Recovery = 63% Analysis Date = 09/25/14 Pct Recovery = 63% Analysis Date = 09/20/14 Pct Recovery = 63% Analysis Date = 09/20/14 Pct Recovery = 63% Analysis Date = 09/15/14 Pct Recovery = 63% Analysis Date = 09/15/14 Pct Recovery = 63% Analysis Date = 09/10/14 Pct Recovery = 63% Analysis Date = 09/10/14 Pct Recovery = 63% Analysis Date = 09/05/14 Pct Recovery = 63% Analysis Date = 09/05/14 Pct Recovery = 63% Analysis Date = 08/31/14 Pct Recovery = 63% Analysis Date = 08/31/14 Pct Recovery = 63% Analysis Date = 08/26/14 Pct Recovery = 62% Analysis Date = 08/26/14 Pct Recovery = 62% Analysis Date = 08/21/14 Pct Recovery = 62% Analysis Date = 08/21/14 Pct Recovery = 62% Analysis Date = 08/16/14 Pct Recovery = 62% Analysis Date = 08/16/14 Pct Recovery = 62% Analysis Date = 08/11/14 Pct Recovery = 62% Analysis Date = 08/11/14 Pct Recovery = 62% Analysis Date = 08/06/14 Pct Recovery = 62% Analysis Date = 08/06/14 Pct Recovery = 62% Analysis Date = 08/01/14 Pct Recovery = 62% Analysis Date = 08/01/14 Pct Recovery = 62% Analysis Date = 07/27/14 Pct Recovery = 62% Analysis Date = 07/27/14 Pct Recovery = 62% Analysis Date = 07/22/14 Pct Recovery = 62% Analysis Date = 07/22/14 Pct Recovery = 62% Analysis Date = 07/17/14 Pct Recovery = 62% Analysis Date = 07/17/14 Pct Recovery = 62% Analysis Date = 07/12/14 Pct Recovery = 62% Analysis Date = 07/12/14 Pct Recovery = 62% Analysis Date = 07/07/14 Pct Recovery = 62% Analysis Date = 07/07/14 Pct Recovery = 62% Analysis Date = 07/02/14 Pct Recovery = 62% Analysis Date = 07/02/14 Pct Recovery = 62% Analysis Date = 06/27/14 Pct Recovery = 62% Analysis Date = 06/27/14 Pct Recovery = 62% Analysis Date = 06/22/14 Pct Recovery = 62% Analysis Date = 06/22/14 Pct Recovery = 62% Analysis Date = 06/17/14 Pct Recovery = 62% Analysis Date = 06/17/14 Pct Recovery = 62% Analysis Date = 06/12/14 Pct Recovery = 61% Analysis Date = 06/12/14 Pct Recovery = 61% Analysis Date = 06/07/14 Pct Recovery = 61% Analysis Date = 06/07/14 Pct Recovery = 61% Analysis Date = 06/02/14 Pct Recovery = 61% Analysis Date = 06/02/14 Pct Recovery = 61% Analysis Date = 05/28/14 Pct Recovery = 61% Analysis Date = 05/28/14 Pct Recovery = 61% Analysis Date = 05/23/14 Pct Recovery = 61% Analysis Date = 05/23/14 Pct Recovery = 61% Analysis Date = 05/18/14 Pct Recovery = 61% Analysis Date = 05/18/14 Pct Recovery = 61% Analysis Date = 05/13/14 Pct Recovery = 61% Analysis Date = 05/13/14 Pct Recovery = 61% Analysis Date = 05/08/14 Pct Recovery = 61% Analysis Date = 05/08/14 Pct Recovery = 61% Analysis Date = 05/03/14 Pct Recovery = 61% Analysis Date = 05/03/14 Pct Recovery = 61% Analysis Date = 04/28/14 Pct Recovery = 61% Analysis Date = 04/28/14 Pct Recovery = 61% Analysis Date = 04/23/14 Pct Recovery = 61% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
QUININE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 77 66% 18% 63% 16%
Total 77 66% 18% 63% 16%

Sample Statistics
QUININE

Characteristic N % % Basis
Plotted 77 99% Spiked
Estimated Values 32 41% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 78 .  
False Negatives 1 1% 1 out of 78
Not Spiked 37 .  
False Positives 0 0% 0 out of 37

BQS OBSP Determination:
RACTOPAMINE
METHOD: 2440 , TESTIDCODE: 52814LCM56
Open Data Set

The SGPlot Procedure

Sample Statistics
RACTOPAMINE

Characteristic N % % Basis
Plotted 0 . Spiked
Estimated Values 0 . Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 . Spiked
Spiked 0 .  
False Negatives 0 . 0 out of 0
Not Spiked 4 .  
False Positives 0 0% 0 out of 4

BQS OBSP Determination:
RALOXIFENE
METHOD: 2440 , TESTIDCODE: 67530LCM56
Open Data Set

Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 242% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 249% Analysis Date = 01/17/16 SpikeMix = ERA 0406-15-09: 80 µl & ERA 0406-15-07A: 80 µl Pct Recovery = 45% Analysis Date = 11/24/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 36% Analysis Date = 10/01/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 12% Analysis Date = 11/05/15 SpikeMix = ERA 0406-15-08: 80 µl & Abs 052215: 80 µl Pct Recovery = 39% Analysis Date = 11/04/15 SpikeMix = Abs 052215: 80 µl & Abs 050115: 80 µl Pct Recovery = 25% Analysis Date = 09/24/16 SpikeMix = Crescent EN160610015: 80 µl & Abs 061416: 80 µl Pct Recovery = 22% Analysis Date = 09/24/16 SpikeMix = Abs 061416: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 23% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 42% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 41% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 25% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 43% Analysis Date = 05/07/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 27% Analysis Date = 04/29/15 SpikeMix = ERA 0319-14-05: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 52% Analysis Date = 01/16/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 24% Analysis Date = 12/07/14 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 13% Analysis Date = 12/06/14 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 15% Analysis Date = 08/28/14 SpikeMix = ERA 0319-14-04: 60 µl & ERA 0319-14-05: 60 µl Pct Recovery = 34% Analysis Date = 07/26/14 SpikeMix = ERA 0319-14-05: 60 µl & ERA 0318-14-02: 60 µl Pct Recovery = 45% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-04: 15 µl & Abs 041814: 15 µl Pct Recovery = 13% Analysis Date = 02/06/15 SpikeMix = Abs 041814: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 18% Analysis Date = 07/12/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 52% Analysis Date = 06/22/14 SpikeMix = Abs 041814: 60 µl & Abs 041614: 60 µl Pct Recovery = 97% Analysis Date = 05/21/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 59% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-08: 40 µl & ERA 0406-15-09: 40 µl Pct Recovery = 31% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-08: 40 µl & Abs 052215: 40 µl Pct Recovery = 51% Analysis Date = 02/23/16 SpikeMix = Abs 052215: 40 µl & Abs 050115: 40 µl Pct Recovery = 51% Analysis Date = 07/31/15 SpikeMix = Abs 051315: 40 µl & Abs 052215: 40 µl Pct Recovery = 52% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 7% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 20% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 14% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 19% Analysis Date = 04/10/15 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 19% Analysis Date = 11/04/14 SpikeMix = Abs 041814: 8 µl & ERA 0318-14-02: 8 µl Pct Recovery = 7% Analysis Date = 10/11/14 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 78% Analysis Date = 08/16/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 35% Analysis Date = 10/10/14 SpikeMix = Abs 041714: 30 µl & Abs 041814: 30 µl Pct Recovery = 102% Analysis Date = 10/10/14 SpikeMix = Abs 041814: 30 µl & ERA 0318-14-02: 30 µl Pct Recovery = 99% Analysis Date = 07/13/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 53% Analysis Date = 05/30/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 72% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 40% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-08: 20 µl & ERA 0406-15-09: 20 µl Pct Recovery = 19% Analysis Date = 11/24/15 SpikeMix = ERA 0406-15-09: 20 µl & Abs 050115: 20 µl Pct Recovery = 30% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 30% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 37% Analysis Date = 02/23/16 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 30% Analysis Date = 11/24/15 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 34% Analysis Date = 07/09/15 SpikeMix = Abs 050115: 20 µl & Abs 052215: 20 µl Pct Recovery = 12% Analysis Date = 06/26/15 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 22% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 41% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 32% Analysis Date = 11/18/16 SpikeMix = ERA 04281604: 80 µl & ERA 04281603: 80 µl Pct Recovery = 28% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & ERA 04281604: 80 µl Pct Recovery = 20% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 66% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 67% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 57% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 62% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 38% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 52% Analysis Date = 01/04/17 Pct Recovery = 51% Analysis Date = 12/31/16 Pct Recovery = 51% Analysis Date = 12/31/16 Pct Recovery = 51% Analysis Date = 12/26/16 Pct Recovery = 51% Analysis Date = 12/26/16 Pct Recovery = 51% Analysis Date = 12/21/16 Pct Recovery = 51% Analysis Date = 12/21/16 Pct Recovery = 51% Analysis Date = 12/16/16 Pct Recovery = 51% Analysis Date = 12/16/16 Pct Recovery = 51% Analysis Date = 12/11/16 Pct Recovery = 51% Analysis Date = 12/11/16 Pct Recovery = 51% Analysis Date = 12/07/16 Pct Recovery = 51% Analysis Date = 12/07/16 Pct Recovery = 51% Analysis Date = 12/02/16 Pct Recovery = 52% Analysis Date = 12/02/16 Pct Recovery = 52% Analysis Date = 11/27/16 Pct Recovery = 52% Analysis Date = 11/27/16 Pct Recovery = 52% Analysis Date = 11/22/16 Pct Recovery = 52% Analysis Date = 11/22/16 Pct Recovery = 52% Analysis Date = 11/17/16 Pct Recovery = 52% Analysis Date = 11/17/16 Pct Recovery = 52% Analysis Date = 11/13/16 Pct Recovery = 52% Analysis Date = 11/13/16 Pct Recovery = 52% Analysis Date = 11/08/16 Pct Recovery = 52% Analysis Date = 11/08/16 Pct Recovery = 52% Analysis Date = 11/03/16 Pct Recovery = 52% Analysis Date = 11/03/16 Pct Recovery = 52% Analysis Date = 10/29/16 Pct Recovery = 52% Analysis Date = 10/29/16 Pct Recovery = 52% Analysis Date = 10/24/16 Pct Recovery = 52% Analysis Date = 10/24/16 Pct Recovery = 52% Analysis Date = 10/20/16 Pct Recovery = 52% Analysis Date = 10/20/16 Pct Recovery = 52% Analysis Date = 10/15/16 Pct Recovery = 52% Analysis Date = 10/15/16 Pct Recovery = 52% Analysis Date = 10/10/16 Pct Recovery = 52% Analysis Date = 10/10/16 Pct Recovery = 52% Analysis Date = 10/05/16 Pct Recovery = 52% Analysis Date = 10/05/16 Pct Recovery = 52% Analysis Date = 09/30/16 Pct Recovery = 52% Analysis Date = 09/30/16 Pct Recovery = 52% Analysis Date = 09/26/16 Pct Recovery = 52% Analysis Date = 09/26/16 Pct Recovery = 52% Analysis Date = 09/21/16 Pct Recovery = 52% Analysis Date = 09/21/16 Pct Recovery = 52% Analysis Date = 09/16/16 Pct Recovery = 52% Analysis Date = 09/16/16 Pct Recovery = 52% Analysis Date = 09/11/16 Pct Recovery = 52% Analysis Date = 09/11/16 Pct Recovery = 52% Analysis Date = 09/06/16 Pct Recovery = 52% Analysis Date = 09/06/16 Pct Recovery = 52% Analysis Date = 09/02/16 Pct Recovery = 52% Analysis Date = 09/02/16 Pct Recovery = 52% Analysis Date = 08/28/16 Pct Recovery = 52% Analysis Date = 08/28/16 Pct Recovery = 52% Analysis Date = 08/23/16 Pct Recovery = 52% Analysis Date = 08/23/16 Pct Recovery = 52% Analysis Date = 08/18/16 Pct Recovery = 52% Analysis Date = 08/18/16 Pct Recovery = 52% Analysis Date = 08/13/16 Pct Recovery = 52% Analysis Date = 08/13/16 Pct Recovery = 52% Analysis Date = 08/09/16 Pct Recovery = 52% Analysis Date = 08/09/16 Pct Recovery = 52% Analysis Date = 08/04/16 Pct Recovery = 51% Analysis Date = 08/04/16 Pct Recovery = 51% Analysis Date = 07/30/16 Pct Recovery = 51% Analysis Date = 07/30/16 Pct Recovery = 51% Analysis Date = 07/25/16 Pct Recovery = 51% Analysis Date = 07/25/16 Pct Recovery = 51% Analysis Date = 07/20/16 Pct Recovery = 51% Analysis Date = 07/20/16 Pct Recovery = 51% Analysis Date = 07/16/16 Pct Recovery = 51% Analysis Date = 07/16/16 Pct Recovery = 51% Analysis Date = 07/11/16 Pct Recovery = 51% Analysis Date = 07/11/16 Pct Recovery = 51% Analysis Date = 07/06/16 Pct Recovery = 51% Analysis Date = 07/06/16 Pct Recovery = 51% Analysis Date = 07/01/16 Pct Recovery = 51% Analysis Date = 07/01/16 Pct Recovery = 51% Analysis Date = 06/26/16 Pct Recovery = 51% Analysis Date = 06/26/16 Pct Recovery = 51% Analysis Date = 06/22/16 Pct Recovery = 51% Analysis Date = 06/22/16 Pct Recovery = 51% Analysis Date = 06/17/16 Pct Recovery = 51% Analysis Date = 06/17/16 Pct Recovery = 51% Analysis Date = 06/12/16 Pct Recovery = 51% Analysis Date = 06/12/16 Pct Recovery = 51% Analysis Date = 06/07/16 Pct Recovery = 50% Analysis Date = 06/07/16 Pct Recovery = 50% Analysis Date = 06/02/16 Pct Recovery = 50% Analysis Date = 06/02/16 Pct Recovery = 50% Analysis Date = 05/29/16 Pct Recovery = 50% Analysis Date = 05/29/16 Pct Recovery = 50% Analysis Date = 05/24/16 Pct Recovery = 50% Analysis Date = 05/24/16 Pct Recovery = 50% Analysis Date = 05/19/16 Pct Recovery = 50% Analysis Date = 05/19/16 Pct Recovery = 50% Analysis Date = 05/14/16 Pct Recovery = 50% Analysis Date = 05/14/16 Pct Recovery = 50% Analysis Date = 05/09/16 Pct Recovery = 50% Analysis Date = 05/09/16 Pct Recovery = 50% Analysis Date = 05/05/16 Pct Recovery = 49% Analysis Date = 05/05/16 Pct Recovery = 49% Analysis Date = 04/30/16 Pct Recovery = 49% Analysis Date = 04/30/16 Pct Recovery = 49% Analysis Date = 04/25/16 Pct Recovery = 49% Analysis Date = 04/25/16 Pct Recovery = 49% Analysis Date = 04/20/16 Pct Recovery = 48% Analysis Date = 04/20/16 Pct Recovery = 48% Analysis Date = 04/15/16 Pct Recovery = 48% Analysis Date = 04/15/16 Pct Recovery = 48% Analysis Date = 04/11/16 Pct Recovery = 47% Analysis Date = 04/11/16 Pct Recovery = 47% Analysis Date = 04/06/16 Pct Recovery = 47% Analysis Date = 04/06/16 Pct Recovery = 47% Analysis Date = 04/01/16 Pct Recovery = 46% Analysis Date = 04/01/16 Pct Recovery = 46% Analysis Date = 03/27/16 Pct Recovery = 46% Analysis Date = 03/27/16 Pct Recovery = 46% Analysis Date = 03/22/16 Pct Recovery = 45% Analysis Date = 03/22/16 Pct Recovery = 45% Analysis Date = 03/18/16 Pct Recovery = 45% Analysis Date = 03/18/16 Pct Recovery = 45% Analysis Date = 03/13/16 Pct Recovery = 44% Analysis Date = 03/13/16 Pct Recovery = 44% Analysis Date = 03/08/16 Pct Recovery = 44% Analysis Date = 03/08/16 Pct Recovery = 44% Analysis Date = 03/03/16 Pct Recovery = 44% Analysis Date = 03/03/16 Pct Recovery = 44% Analysis Date = 02/27/16 Pct Recovery = 43% Analysis Date = 02/27/16 Pct Recovery = 43% Analysis Date = 02/23/16 Pct Recovery = 43% Analysis Date = 02/23/16 Pct Recovery = 43% Analysis Date = 02/18/16 Pct Recovery = 42% Analysis Date = 02/18/16 Pct Recovery = 42% Analysis Date = 02/13/16 Pct Recovery = 42% Analysis Date = 02/13/16 Pct Recovery = 42% Analysis Date = 02/08/16 Pct Recovery = 41% Analysis Date = 02/08/16 Pct Recovery = 41% Analysis Date = 02/03/16 Pct Recovery = 41% Analysis Date = 02/03/16 Pct Recovery = 41% Analysis Date = 01/30/16 Pct Recovery = 40% Analysis Date = 01/30/16 Pct Recovery = 40% Analysis Date = 01/25/16 Pct Recovery = 40% Analysis Date = 01/25/16 Pct Recovery = 40% Analysis Date = 01/20/16 Pct Recovery = 39% Analysis Date = 01/20/16 Pct Recovery = 39% Analysis Date = 01/15/16 Pct Recovery = 39% Analysis Date = 01/15/16 Pct Recovery = 39% Analysis Date = 01/10/16 Pct Recovery = 39% Analysis Date = 01/10/16 Pct Recovery = 39% Analysis Date = 01/06/16 Pct Recovery = 38% Analysis Date = 01/06/16 Pct Recovery = 38% Analysis Date = 01/01/16 Pct Recovery = 38% Analysis Date = 01/01/16 Pct Recovery = 38% Analysis Date = 12/27/15 Pct Recovery = 37% Analysis Date = 12/27/15 Pct Recovery = 37% Analysis Date = 12/22/15 Pct Recovery = 37% Analysis Date = 12/22/15 Pct Recovery = 37% Analysis Date = 12/17/15 Pct Recovery = 36% Analysis Date = 12/17/15 Pct Recovery = 36% Analysis Date = 12/13/15 Pct Recovery = 36% Analysis Date = 12/13/15 Pct Recovery = 36% Analysis Date = 12/08/15 Pct Recovery = 35% Analysis Date = 12/08/15 Pct Recovery = 35% Analysis Date = 12/03/15 Pct Recovery = 35% Analysis Date = 12/03/15 Pct Recovery = 35% Analysis Date = 11/28/15 Pct Recovery = 35% Analysis Date = 11/28/15 Pct Recovery = 35% Analysis Date = 11/23/15 Pct Recovery = 34% Analysis Date = 11/23/15 Pct Recovery = 34% Analysis Date = 11/19/15 Pct Recovery = 34% Analysis Date = 11/19/15 Pct Recovery = 34% Analysis Date = 11/14/15 Pct Recovery = 34% Analysis Date = 11/14/15 Pct Recovery = 34% Analysis Date = 11/09/15 Pct Recovery = 34% Analysis Date = 11/09/15 Pct Recovery = 34% Analysis Date = 11/04/15 Pct Recovery = 33% Analysis Date = 11/04/15 Pct Recovery = 33% Analysis Date = 10/30/15 Pct Recovery = 33% Analysis Date = 10/30/15 Pct Recovery = 33% Analysis Date = 10/26/15 Pct Recovery = 33% Analysis Date = 10/26/15 Pct Recovery = 33% Analysis Date = 10/21/15 Pct Recovery = 33% Analysis Date = 10/21/15 Pct Recovery = 33% Analysis Date = 10/16/15 Pct Recovery = 33% Analysis Date = 10/16/15 Pct Recovery = 33% Analysis Date = 10/11/15 Pct Recovery = 32% Analysis Date = 10/11/15 Pct Recovery = 32% Analysis Date = 10/06/15 Pct Recovery = 32% Analysis Date = 10/06/15 Pct Recovery = 32% Analysis Date = 10/02/15 Pct Recovery = 32% Analysis Date = 10/02/15 Pct Recovery = 32% Analysis Date = 09/27/15 Pct Recovery = 32% Analysis Date = 09/27/15 Pct Recovery = 32% Analysis Date = 09/22/15 Pct Recovery = 32% Analysis Date = 09/22/15 Pct Recovery = 32% Analysis Date = 09/17/15 Pct Recovery = 32% Analysis Date = 09/17/15 Pct Recovery = 32% Analysis Date = 09/12/15 Pct Recovery = 31% Analysis Date = 09/12/15 Pct Recovery = 31% Analysis Date = 09/08/15 Pct Recovery = 31% Analysis Date = 09/08/15 Pct Recovery = 31% Analysis Date = 09/03/15 Pct Recovery = 31% Analysis Date = 09/03/15 Pct Recovery = 31% Analysis Date = 08/29/15 Pct Recovery = 31% Analysis Date = 08/29/15 Pct Recovery = 31% Analysis Date = 08/24/15 Pct Recovery = 31% Analysis Date = 08/24/15 Pct Recovery = 31% Analysis Date = 08/19/15 Pct Recovery = 30% Analysis Date = 08/19/15 Pct Recovery = 30% Analysis Date = 08/15/15 Pct Recovery = 30% Analysis Date = 08/15/15 Pct Recovery = 30% Analysis Date = 08/10/15 Pct Recovery = 30% Analysis Date = 08/10/15 Pct Recovery = 30% Analysis Date = 08/05/15 Pct Recovery = 30% Analysis Date = 08/05/15 Pct Recovery = 30% Analysis Date = 07/31/15 Pct Recovery = 30% Analysis Date = 07/31/15 Pct Recovery = 30% Analysis Date = 07/26/15 Pct Recovery = 30% Analysis Date = 07/26/15 Pct Recovery = 30% Analysis Date = 07/22/15 Pct Recovery = 30% Analysis Date = 07/22/15 Pct Recovery = 30% Analysis Date = 07/17/15 Pct Recovery = 30% Analysis Date = 07/17/15 Pct Recovery = 30% Analysis Date = 07/12/15 Pct Recovery = 30% Analysis Date = 07/12/15 Pct Recovery = 30% Analysis Date = 07/07/15 Pct Recovery = 30% Analysis Date = 07/07/15 Pct Recovery = 30% Analysis Date = 07/02/15 Pct Recovery = 30% Analysis Date = 07/02/15 Pct Recovery = 30% Analysis Date = 06/28/15 Pct Recovery = 30% Analysis Date = 06/28/15 Pct Recovery = 30% Analysis Date = 06/23/15 Pct Recovery = 30% Analysis Date = 06/23/15 Pct Recovery = 30% Analysis Date = 06/18/15 Pct Recovery = 31% Analysis Date = 06/18/15 Pct Recovery = 31% Analysis Date = 06/13/15 Pct Recovery = 31% Analysis Date = 06/13/15 Pct Recovery = 31% Analysis Date = 06/08/15 Pct Recovery = 31% Analysis Date = 06/08/15 Pct Recovery = 31% Analysis Date = 06/04/15 Pct Recovery = 31% Analysis Date = 06/04/15 Pct Recovery = 31% Analysis Date = 05/30/15 Pct Recovery = 31% Analysis Date = 05/30/15 Pct Recovery = 31% Analysis Date = 05/25/15 Pct Recovery = 31% Analysis Date = 05/25/15 Pct Recovery = 31% Analysis Date = 05/20/15 Pct Recovery = 31% Analysis Date = 05/20/15 Pct Recovery = 31% Analysis Date = 05/15/15 Pct Recovery = 31% Analysis Date = 05/15/15 Pct Recovery = 31% Analysis Date = 05/11/15 Pct Recovery = 31% Analysis Date = 05/11/15 Pct Recovery = 31% Analysis Date = 05/06/15 Pct Recovery = 31% Analysis Date = 05/06/15 Pct Recovery = 31% Analysis Date = 05/01/15 Pct Recovery = 32% Analysis Date = 05/01/15 Pct Recovery = 32% Analysis Date = 04/26/15 Pct Recovery = 32% Analysis Date = 04/26/15 Pct Recovery = 32% Analysis Date = 04/21/15 Pct Recovery = 32% Analysis Date = 04/21/15 Pct Recovery = 32% Analysis Date = 04/17/15 Pct Recovery = 33% Analysis Date = 04/17/15 Pct Recovery = 33% Analysis Date = 04/12/15 Pct Recovery = 33% Analysis Date = 04/12/15 Pct Recovery = 33% Analysis Date = 04/07/15 Pct Recovery = 33% Analysis Date = 04/07/15 Pct Recovery = 33% Analysis Date = 04/02/15 Pct Recovery = 34% Analysis Date = 04/02/15 Pct Recovery = 34% Analysis Date = 03/28/15 Pct Recovery = 34% Analysis Date = 03/28/15 Pct Recovery = 34% Analysis Date = 03/24/15 Pct Recovery = 34% Analysis Date = 03/24/15 Pct Recovery = 34% Analysis Date = 03/19/15 Pct Recovery = 35% Analysis Date = 03/19/15 Pct Recovery = 35% Analysis Date = 03/14/15 Pct Recovery = 35% Analysis Date = 03/14/15 Pct Recovery = 35% Analysis Date = 03/09/15 Pct Recovery = 36% Analysis Date = 03/09/15 Pct Recovery = 36% Analysis Date = 03/04/15 Pct Recovery = 36% Analysis Date = 03/04/15 Pct Recovery = 36% Analysis Date = 02/28/15 Pct Recovery = 36% Analysis Date = 02/28/15 Pct Recovery = 36% Analysis Date = 02/23/15 Pct Recovery = 37% Analysis Date = 02/23/15 Pct Recovery = 37% Analysis Date = 02/18/15 Pct Recovery = 37% Analysis Date = 02/18/15 Pct Recovery = 37% Analysis Date = 02/13/15 Pct Recovery = 38% Analysis Date = 02/13/15 Pct Recovery = 38% Analysis Date = 02/08/15 Pct Recovery = 38% Analysis Date = 02/08/15 Pct Recovery = 38% Analysis Date = 02/04/15 Pct Recovery = 38% Analysis Date = 02/04/15 Pct Recovery = 38% Analysis Date = 01/30/15 Pct Recovery = 39% Analysis Date = 01/30/15 Pct Recovery = 39% Analysis Date = 01/25/15 Pct Recovery = 39% Analysis Date = 01/25/15 Pct Recovery = 39% Analysis Date = 01/20/15 Pct Recovery = 39% Analysis Date = 01/20/15 Pct Recovery = 39% Analysis Date = 01/15/15 Pct Recovery = 40% Analysis Date = 01/15/15 Pct Recovery = 40% Analysis Date = 01/11/15 Pct Recovery = 40% Analysis Date = 01/11/15 Pct Recovery = 40% Analysis Date = 01/06/15 Pct Recovery = 41% Analysis Date = 01/06/15 Pct Recovery = 41% Analysis Date = 01/01/15 Pct Recovery = 41% Analysis Date = 01/01/15 Pct Recovery = 41% Analysis Date = 12/27/14 Pct Recovery = 42% Analysis Date = 12/27/14 Pct Recovery = 42% Analysis Date = 12/22/14 Pct Recovery = 42% Analysis Date = 12/22/14 Pct Recovery = 42% Analysis Date = 12/18/14 Pct Recovery = 43% Analysis Date = 12/18/14 Pct Recovery = 43% Analysis Date = 12/13/14 Pct Recovery = 43% Analysis Date = 12/13/14 Pct Recovery = 43% Analysis Date = 12/08/14 Pct Recovery = 43% Analysis Date = 12/08/14 Pct Recovery = 43% Analysis Date = 12/03/14 Pct Recovery = 44% Analysis Date = 12/03/14 Pct Recovery = 44% Analysis Date = 11/28/14 Pct Recovery = 44% Analysis Date = 11/28/14 Pct Recovery = 44% Analysis Date = 11/24/14 Pct Recovery = 45% Analysis Date = 11/24/14 Pct Recovery = 45% Analysis Date = 11/19/14 Pct Recovery = 45% Analysis Date = 11/19/14 Pct Recovery = 45% Analysis Date = 11/14/14 Pct Recovery = 46% Analysis Date = 11/14/14 Pct Recovery = 46% Analysis Date = 11/09/14 Pct Recovery = 46% Analysis Date = 11/09/14 Pct Recovery = 46% Analysis Date = 11/04/14 Pct Recovery = 47% Analysis Date = 11/04/14 Pct Recovery = 47% Analysis Date = 10/31/14 Pct Recovery = 47% Analysis Date = 10/31/14 Pct Recovery = 47% Analysis Date = 10/26/14 Pct Recovery = 48% Analysis Date = 10/26/14 Pct Recovery = 48% Analysis Date = 10/21/14 Pct Recovery = 48% Analysis Date = 10/21/14 Pct Recovery = 48% Analysis Date = 10/16/14 Pct Recovery = 49% Analysis Date = 10/16/14 Pct Recovery = 49% Analysis Date = 10/11/14 Pct Recovery = 49% Analysis Date = 10/11/14 Pct Recovery = 49% Analysis Date = 10/07/14 Pct Recovery = 49% Analysis Date = 10/07/14 Pct Recovery = 49% Analysis Date = 10/02/14 Pct Recovery = 50% Analysis Date = 10/02/14 Pct Recovery = 50% Analysis Date = 09/27/14 Pct Recovery = 50% Analysis Date = 09/27/14 Pct Recovery = 50% Analysis Date = 09/22/14 Pct Recovery = 51% Analysis Date = 09/22/14 Pct Recovery = 51% Analysis Date = 09/17/14 Pct Recovery = 51% Analysis Date = 09/17/14 Pct Recovery = 51% Analysis Date = 09/13/14 Pct Recovery = 52% Analysis Date = 09/13/14 Pct Recovery = 52% Analysis Date = 09/08/14 Pct Recovery = 52% Analysis Date = 09/08/14 Pct Recovery = 52% Analysis Date = 09/03/14 Pct Recovery = 53% Analysis Date = 09/03/14 Pct Recovery = 53% Analysis Date = 08/29/14 Pct Recovery = 53% Analysis Date = 08/29/14 Pct Recovery = 53% Analysis Date = 08/24/14 Pct Recovery = 54% Analysis Date = 08/24/14 Pct Recovery = 54% Analysis Date = 08/20/14 Pct Recovery = 54% Analysis Date = 08/20/14 Pct Recovery = 54% Analysis Date = 08/15/14 Pct Recovery = 55% Analysis Date = 08/15/14 Pct Recovery = 55% Analysis Date = 08/10/14 Pct Recovery = 55% Analysis Date = 08/10/14 Pct Recovery = 55% Analysis Date = 08/05/14 Pct Recovery = 56% Analysis Date = 08/05/14 Pct Recovery = 56% Analysis Date = 07/31/14 Pct Recovery = 56% Analysis Date = 07/31/14 Pct Recovery = 56% Analysis Date = 07/27/14 Pct Recovery = 57% Analysis Date = 07/27/14 Pct Recovery = 57% Analysis Date = 07/22/14 Pct Recovery = 57% Analysis Date = 07/22/14 Pct Recovery = 57% Analysis Date = 07/17/14 Pct Recovery = 58% Analysis Date = 07/17/14 Pct Recovery = 58% Analysis Date = 07/12/14 Pct Recovery = 58% Analysis Date = 07/12/14 Pct Recovery = 58% Analysis Date = 07/07/14 Pct Recovery = 59% Analysis Date = 07/07/14 Pct Recovery = 59% Analysis Date = 07/03/14 Pct Recovery = 59% Analysis Date = 07/03/14 Pct Recovery = 59% Analysis Date = 06/28/14 Pct Recovery = 60% Analysis Date = 06/28/14 Pct Recovery = 60% Analysis Date = 06/23/14 Pct Recovery = 60% Analysis Date = 06/23/14 Pct Recovery = 60% Analysis Date = 06/18/14 Pct Recovery = 61% Analysis Date = 06/18/14 Pct Recovery = 61% Analysis Date = 06/13/14 Pct Recovery = 62% Analysis Date = 06/13/14 Pct Recovery = 62% Analysis Date = 06/09/14 Pct Recovery = 62% Analysis Date = 06/09/14 Pct Recovery = 62% Analysis Date = 06/04/14 Pct Recovery = 63% Analysis Date = 06/04/14 Pct Recovery = 63% Analysis Date = 05/30/14 Pct Recovery = 63% Analysis Date = 05/30/14 Pct Recovery = 63% Analysis Date = 05/25/14 Pct Recovery = 64% Analysis Date = 05/25/14 Pct Recovery = 64% Analysis Date = 05/21/14 Pct Recovery = 64% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
RALOXIFENE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 10 46% 17% 46% 22%
>= Reporting Level 50 45% 47% 34% 23%
Total 60 45% 43% 36% 22%

Sample Statistics
RALOXIFENE

Characteristic N % % Basis
Plotted 60 80% Spiked
Estimated Values 60 80% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 4 5% Spiked
Spiked 75 .  
False Negatives 11 15% 11 out of 75
Not Spiked 40 .  
False Positives 0 0% 0 out of 40

BQS OBSP Determination:
RANITIDINE
METHOD: 2440 , TESTIDCODE: 67452LCM56
Open Data Set

Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 44% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 48% Analysis Date = 11/24/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 62% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 80 µl & Abs 051315: 80 µl Pct Recovery = 11% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 80 µl & ERA 0406-15-08: 80 µl Pct Recovery = 13% Analysis Date = 11/05/15 SpikeMix = ERA 0406-15-08: 80 µl & Abs 052215: 80 µl Pct Recovery = 43% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 1% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 1% Analysis Date = 11/18/16 SpikeMix = ERA 04281604: 80 µl & ERA 04281603: 80 µl Pct Recovery = 50% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & ERA 04281604: 80 µl Pct Recovery = 48% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 54% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 43% Analysis Date = 05/07/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 16% Analysis Date = 04/29/15 SpikeMix = ERA 0319-14-05: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 71% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 39% Analysis Date = 01/16/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 40% Analysis Date = 12/07/14 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 26% Analysis Date = 12/06/14 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 9% Analysis Date = 08/28/14 SpikeMix = ERA 0319-14-04: 60 µl & ERA 0319-14-05: 60 µl Pct Recovery = 39% Analysis Date = 07/26/14 SpikeMix = ERA 0319-14-05: 60 µl & ERA 0318-14-02: 60 µl Pct Recovery = 43% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-04: 15 µl & Abs 041814: 15 µl Pct Recovery = 44% Analysis Date = 07/12/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 22% Analysis Date = 06/22/14 SpikeMix = Abs 041814: 60 µl & Abs 041614: 60 µl Pct Recovery = 57% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-08: 40 µl & Abs 052215: 40 µl Pct Recovery = 42% Analysis Date = 11/04/15 SpikeMix = ERA 0406-15-07A: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 31% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-08: 40 µl & ERA 0406-15-09: 40 µl Pct Recovery = 24% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 32% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 56% Analysis Date = 11/04/14 SpikeMix = Abs 041714: 8 µl & ERA 0319-14-05: 8 µl Pct Recovery = 19% Analysis Date = 10/24/14 SpikeMix = ERA 0319-14-05: 8 µl & Abs 041614: 8 µl Pct Recovery = 16% Analysis Date = 04/10/15 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 54% Analysis Date = 11/04/14 SpikeMix = Abs 041814: 8 µl & ERA 0318-14-02: 8 µl Pct Recovery = 34% Analysis Date = 08/30/14 SpikeMix = ERA 0318-14-02: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 36% Analysis Date = 08/16/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 19% Analysis Date = 07/13/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 7% Analysis Date = 07/13/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 42% Analysis Date = 04/23/14 SpikeMix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.2: 20 µl Pct Recovery = 14% Analysis Date = 06/26/15 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 42% Analysis Date = 04/27/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 65% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 25% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-08: 20 µl & ERA 0406-15-09: 20 µl Pct Recovery = 40% Analysis Date = 11/25/15 SpikeMix = Abs 050115: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 4% Analysis Date = 09/15/15 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 45% Analysis Date = 09/09/15 SpikeMix = ERA 0406-15-08: 20 µl & Abs 052215: 20 µl Pct Recovery = 10% Analysis Date = 01/18/17 Pct Recovery = 42% Analysis Date = 01/13/17 Pct Recovery = 42% Analysis Date = 01/13/17 Pct Recovery = 42% Analysis Date = 01/08/17 Pct Recovery = 42% Analysis Date = 01/08/17 Pct Recovery = 42% Analysis Date = 01/03/17 Pct Recovery = 42% Analysis Date = 01/03/17 Pct Recovery = 42% Analysis Date = 12/29/16 Pct Recovery = 42% Analysis Date = 12/29/16 Pct Recovery = 42% Analysis Date = 12/24/16 Pct Recovery = 41% Analysis Date = 12/24/16 Pct Recovery = 41% Analysis Date = 12/19/16 Pct Recovery = 41% Analysis Date = 12/19/16 Pct Recovery = 41% Analysis Date = 12/14/16 Pct Recovery = 41% Analysis Date = 12/14/16 Pct Recovery = 41% Analysis Date = 12/09/16 Pct Recovery = 41% Analysis Date = 12/09/16 Pct Recovery = 41% Analysis Date = 12/04/16 Pct Recovery = 41% Analysis Date = 12/04/16 Pct Recovery = 41% Analysis Date = 11/29/16 Pct Recovery = 41% Analysis Date = 11/29/16 Pct Recovery = 41% Analysis Date = 11/24/16 Pct Recovery = 41% Analysis Date = 11/24/16 Pct Recovery = 41% Analysis Date = 11/19/16 Pct Recovery = 40% Analysis Date = 11/19/16 Pct Recovery = 40% Analysis Date = 11/14/16 Pct Recovery = 40% Analysis Date = 11/14/16 Pct Recovery = 40% Analysis Date = 11/09/16 Pct Recovery = 40% Analysis Date = 11/09/16 Pct Recovery = 40% Analysis Date = 11/04/16 Pct Recovery = 40% Analysis Date = 11/04/16 Pct Recovery = 40% Analysis Date = 10/30/16 Pct Recovery = 40% Analysis Date = 10/30/16 Pct Recovery = 40% Analysis Date = 10/25/16 Pct Recovery = 40% Analysis Date = 10/25/16 Pct Recovery = 40% Analysis Date = 10/20/16 Pct Recovery = 39% Analysis Date = 10/20/16 Pct Recovery = 39% Analysis Date = 10/15/16 Pct Recovery = 39% Analysis Date = 10/15/16 Pct Recovery = 39% Analysis Date = 10/10/16 Pct Recovery = 39% Analysis Date = 10/10/16 Pct Recovery = 39% Analysis Date = 10/05/16 Pct Recovery = 39% Analysis Date = 10/05/16 Pct Recovery = 39% Analysis Date = 09/30/16 Pct Recovery = 39% Analysis Date = 09/30/16 Pct Recovery = 39% Analysis Date = 09/25/16 Pct Recovery = 39% Analysis Date = 09/25/16 Pct Recovery = 39% Analysis Date = 09/20/16 Pct Recovery = 39% Analysis Date = 09/20/16 Pct Recovery = 39% Analysis Date = 09/15/16 Pct Recovery = 38% Analysis Date = 09/15/16 Pct Recovery = 38% Analysis Date = 09/10/16 Pct Recovery = 38% Analysis Date = 09/10/16 Pct Recovery = 38% Analysis Date = 09/05/16 Pct Recovery = 38% Analysis Date = 09/05/16 Pct Recovery = 38% Analysis Date = 08/31/16 Pct Recovery = 38% Analysis Date = 08/31/16 Pct Recovery = 38% Analysis Date = 08/26/16 Pct Recovery = 38% Analysis Date = 08/26/16 Pct Recovery = 38% Analysis Date = 08/21/16 Pct Recovery = 38% Analysis Date = 08/21/16 Pct Recovery = 38% Analysis Date = 08/16/16 Pct Recovery = 37% Analysis Date = 08/16/16 Pct Recovery = 37% Analysis Date = 08/11/16 Pct Recovery = 37% Analysis Date = 08/11/16 Pct Recovery = 37% Analysis Date = 08/06/16 Pct Recovery = 37% Analysis Date = 08/06/16 Pct Recovery = 37% Analysis Date = 08/01/16 Pct Recovery = 37% Analysis Date = 08/01/16 Pct Recovery = 37% Analysis Date = 07/27/16 Pct Recovery = 37% Analysis Date = 07/27/16 Pct Recovery = 37% Analysis Date = 07/22/16 Pct Recovery = 37% Analysis Date = 07/22/16 Pct Recovery = 37% Analysis Date = 07/17/16 Pct Recovery = 36% Analysis Date = 07/17/16 Pct Recovery = 36% Analysis Date = 07/12/16 Pct Recovery = 36% Analysis Date = 07/12/16 Pct Recovery = 36% Analysis Date = 07/07/16 Pct Recovery = 36% Analysis Date = 07/07/16 Pct Recovery = 36% Analysis Date = 07/02/16 Pct Recovery = 36% Analysis Date = 07/02/16 Pct Recovery = 36% Analysis Date = 06/27/16 Pct Recovery = 36% Analysis Date = 06/27/16 Pct Recovery = 36% Analysis Date = 06/22/16 Pct Recovery = 36% Analysis Date = 06/22/16 Pct Recovery = 36% Analysis Date = 06/17/16 Pct Recovery = 35% Analysis Date = 06/17/16 Pct Recovery = 35% Analysis Date = 06/12/16 Pct Recovery = 35% Analysis Date = 06/12/16 Pct Recovery = 35% Analysis Date = 06/07/16 Pct Recovery = 35% Analysis Date = 06/07/16 Pct Recovery = 35% Analysis Date = 06/02/16 Pct Recovery = 35% Analysis Date = 06/02/16 Pct Recovery = 35% Analysis Date = 05/28/16 Pct Recovery = 35% Analysis Date = 05/28/16 Pct Recovery = 35% Analysis Date = 05/23/16 Pct Recovery = 35% Analysis Date = 05/23/16 Pct Recovery = 35% Analysis Date = 05/18/16 Pct Recovery = 34% Analysis Date = 05/18/16 Pct Recovery = 34% Analysis Date = 05/13/16 Pct Recovery = 34% Analysis Date = 05/13/16 Pct Recovery = 34% Analysis Date = 05/08/16 Pct Recovery = 34% Analysis Date = 05/08/16 Pct Recovery = 34% Analysis Date = 05/03/16 Pct Recovery = 34% Analysis Date = 05/03/16 Pct Recovery = 34% Analysis Date = 04/28/16 Pct Recovery = 34% Analysis Date = 04/28/16 Pct Recovery = 34% Analysis Date = 04/23/16 Pct Recovery = 34% Analysis Date = 04/23/16 Pct Recovery = 34% Analysis Date = 04/18/16 Pct Recovery = 33% Analysis Date = 04/18/16 Pct Recovery = 33% Analysis Date = 04/13/16 Pct Recovery = 33% Analysis Date = 04/13/16 Pct Recovery = 33% Analysis Date = 04/08/16 Pct Recovery = 33% Analysis Date = 04/08/16 Pct Recovery = 33% Analysis Date = 04/03/16 Pct Recovery = 33% Analysis Date = 04/03/16 Pct Recovery = 33% Analysis Date = 03/29/16 Pct Recovery = 33% Analysis Date = 03/29/16 Pct Recovery = 33% Analysis Date = 03/24/16 Pct Recovery = 33% Analysis Date = 03/24/16 Pct Recovery = 33% Analysis Date = 03/19/16 Pct Recovery = 33% Analysis Date = 03/19/16 Pct Recovery = 33% Analysis Date = 03/14/16 Pct Recovery = 33% Analysis Date = 03/14/16 Pct Recovery = 33% Analysis Date = 03/09/16 Pct Recovery = 33% Analysis Date = 03/09/16 Pct Recovery = 33% Analysis Date = 03/04/16 Pct Recovery = 33% Analysis Date = 03/04/16 Pct Recovery = 33% Analysis Date = 02/28/16 Pct Recovery = 33% Analysis Date = 02/28/16 Pct Recovery = 33% Analysis Date = 02/23/16 Pct Recovery = 33% Analysis Date = 02/23/16 Pct Recovery = 33% Analysis Date = 02/18/16 Pct Recovery = 33% Analysis Date = 02/18/16 Pct Recovery = 33% Analysis Date = 02/13/16 Pct Recovery = 33% Analysis Date = 02/13/16 Pct Recovery = 33% Analysis Date = 02/08/16 Pct Recovery = 33% Analysis Date = 02/08/16 Pct Recovery = 33% Analysis Date = 02/03/16 Pct Recovery = 33% Analysis Date = 02/03/16 Pct Recovery = 33% Analysis Date = 01/29/16 Pct Recovery = 33% Analysis Date = 01/29/16 Pct Recovery = 33% Analysis Date = 01/24/16 Pct Recovery = 33% Analysis Date = 01/24/16 Pct Recovery = 33% Analysis Date = 01/19/16 Pct Recovery = 33% Analysis Date = 01/19/16 Pct Recovery = 33% Analysis Date = 01/14/16 Pct Recovery = 33% Analysis Date = 01/14/16 Pct Recovery = 33% Analysis Date = 01/09/16 Pct Recovery = 33% Analysis Date = 01/09/16 Pct Recovery = 33% Analysis Date = 01/04/16 Pct Recovery = 33% Analysis Date = 01/04/16 Pct Recovery = 33% Analysis Date = 12/30/15 Pct Recovery = 33% Analysis Date = 12/30/15 Pct Recovery = 33% Analysis Date = 12/25/15 Pct Recovery = 33% Analysis Date = 12/25/15 Pct Recovery = 33% Analysis Date = 12/20/15 Pct Recovery = 33% Analysis Date = 12/20/15 Pct Recovery = 33% Analysis Date = 12/15/15 Pct Recovery = 33% Analysis Date = 12/15/15 Pct Recovery = 33% Analysis Date = 12/10/15 Pct Recovery = 33% Analysis Date = 12/10/15 Pct Recovery = 33% Analysis Date = 12/05/15 Pct Recovery = 33% Analysis Date = 12/05/15 Pct Recovery = 33% Analysis Date = 11/30/15 Pct Recovery = 33% Analysis Date = 11/30/15 Pct Recovery = 33% Analysis Date = 11/25/15 Pct Recovery = 33% Analysis Date = 11/25/15 Pct Recovery = 33% Analysis Date = 11/20/15 Pct Recovery = 33% Analysis Date = 11/20/15 Pct Recovery = 33% Analysis Date = 11/15/15 Pct Recovery = 33% Analysis Date = 11/15/15 Pct Recovery = 33% Analysis Date = 11/10/15 Pct Recovery = 33% Analysis Date = 11/10/15 Pct Recovery = 33% Analysis Date = 11/05/15 Pct Recovery = 34% Analysis Date = 11/05/15 Pct Recovery = 34% Analysis Date = 10/31/15 Pct Recovery = 34% Analysis Date = 10/31/15 Pct Recovery = 34% Analysis Date = 10/26/15 Pct Recovery = 34% Analysis Date = 10/26/15 Pct Recovery = 34% Analysis Date = 10/21/15 Pct Recovery = 34% Analysis Date = 10/21/15 Pct Recovery = 34% Analysis Date = 10/16/15 Pct Recovery = 34% Analysis Date = 10/16/15 Pct Recovery = 34% Analysis Date = 10/11/15 Pct Recovery = 34% Analysis Date = 10/11/15 Pct Recovery = 34% Analysis Date = 10/06/15 Pct Recovery = 34% Analysis Date = 10/06/15 Pct Recovery = 34% Analysis Date = 10/01/15 Pct Recovery = 34% Analysis Date = 10/01/15 Pct Recovery = 34% Analysis Date = 09/26/15 Pct Recovery = 34% Analysis Date = 09/26/15 Pct Recovery = 34% Analysis Date = 09/21/15 Pct Recovery = 34% Analysis Date = 09/21/15 Pct Recovery = 34% Analysis Date = 09/16/15 Pct Recovery = 34% Analysis Date = 09/16/15 Pct Recovery = 34% Analysis Date = 09/11/15 Pct Recovery = 34% Analysis Date = 09/11/15 Pct Recovery = 34% Analysis Date = 09/05/15 Pct Recovery = 34% Analysis Date = 09/05/15 Pct Recovery = 34% Analysis Date = 08/31/15 Pct Recovery = 34% Analysis Date = 08/31/15 Pct Recovery = 34% Analysis Date = 08/26/15 Pct Recovery = 34% Analysis Date = 08/26/15 Pct Recovery = 34% Analysis Date = 08/21/15 Pct Recovery = 35% Analysis Date = 08/21/15 Pct Recovery = 35% Analysis Date = 08/16/15 Pct Recovery = 35% Analysis Date = 08/16/15 Pct Recovery = 35% Analysis Date = 08/11/15 Pct Recovery = 35% Analysis Date = 08/11/15 Pct Recovery = 35% Analysis Date = 08/06/15 Pct Recovery = 35% Analysis Date = 08/06/15 Pct Recovery = 35% Analysis Date = 08/01/15 Pct Recovery = 35% Analysis Date = 08/01/15 Pct Recovery = 35% Analysis Date = 07/27/15 Pct Recovery = 35% Analysis Date = 07/27/15 Pct Recovery = 35% Analysis Date = 07/22/15 Pct Recovery = 35% Analysis Date = 07/22/15 Pct Recovery = 35% Analysis Date = 07/17/15 Pct Recovery = 35% Analysis Date = 07/17/15 Pct Recovery = 35% Analysis Date = 07/12/15 Pct Recovery = 35% Analysis Date = 07/12/15 Pct Recovery = 35% Analysis Date = 07/07/15 Pct Recovery = 35% Analysis Date = 07/07/15 Pct Recovery = 35% Analysis Date = 07/02/15 Pct Recovery = 35% Analysis Date = 07/02/15 Pct Recovery = 35% Analysis Date = 06/27/15 Pct Recovery = 35% Analysis Date = 06/27/15 Pct Recovery = 35% Analysis Date = 06/22/15 Pct Recovery = 35% Analysis Date = 06/22/15 Pct Recovery = 35% Analysis Date = 06/17/15 Pct Recovery = 35% Analysis Date = 06/17/15 Pct Recovery = 35% Analysis Date = 06/12/15 Pct Recovery = 35% Analysis Date = 06/12/15 Pct Recovery = 35% Analysis Date = 06/07/15 Pct Recovery = 35% Analysis Date = 06/07/15 Pct Recovery = 35% Analysis Date = 06/02/15 Pct Recovery = 35% Analysis Date = 06/02/15 Pct Recovery = 35% Analysis Date = 05/28/15 Pct Recovery = 35% Analysis Date = 05/28/15 Pct Recovery = 35% Analysis Date = 05/23/15 Pct Recovery = 35% Analysis Date = 05/23/15 Pct Recovery = 35% Analysis Date = 05/18/15 Pct Recovery = 35% Analysis Date = 05/18/15 Pct Recovery = 35% Analysis Date = 05/13/15 Pct Recovery = 35% Analysis Date = 05/13/15 Pct Recovery = 35% Analysis Date = 05/08/15 Pct Recovery = 35% Analysis Date = 05/08/15 Pct Recovery = 35% Analysis Date = 05/03/15 Pct Recovery = 35% Analysis Date = 05/03/15 Pct Recovery = 35% Analysis Date = 04/28/15 Pct Recovery = 35% Analysis Date = 04/28/15 Pct Recovery = 35% Analysis Date = 04/23/15 Pct Recovery = 35% Analysis Date = 04/23/15 Pct Recovery = 35% Analysis Date = 04/18/15 Pct Recovery = 35% Analysis Date = 04/18/15 Pct Recovery = 35% Analysis Date = 04/13/15 Pct Recovery = 35% Analysis Date = 04/13/15 Pct Recovery = 35% Analysis Date = 04/08/15 Pct Recovery = 35% Analysis Date = 04/08/15 Pct Recovery = 35% Analysis Date = 04/03/15 Pct Recovery = 35% Analysis Date = 04/03/15 Pct Recovery = 35% Analysis Date = 03/29/15 Pct Recovery = 36% Analysis Date = 03/29/15 Pct Recovery = 36% Analysis Date = 03/24/15 Pct Recovery = 36% Analysis Date = 03/24/15 Pct Recovery = 36% Analysis Date = 03/19/15 Pct Recovery = 36% Analysis Date = 03/19/15 Pct Recovery = 36% Analysis Date = 03/14/15 Pct Recovery = 36% Analysis Date = 03/14/15 Pct Recovery = 36% Analysis Date = 03/09/15 Pct Recovery = 36% Analysis Date = 03/09/15 Pct Recovery = 36% Analysis Date = 03/04/15 Pct Recovery = 36% Analysis Date = 03/04/15 Pct Recovery = 36% Analysis Date = 02/27/15 Pct Recovery = 35% Analysis Date = 02/27/15 Pct Recovery = 35% Analysis Date = 02/22/15 Pct Recovery = 35% Analysis Date = 02/22/15 Pct Recovery = 35% Analysis Date = 02/17/15 Pct Recovery = 35% Analysis Date = 02/17/15 Pct Recovery = 35% Analysis Date = 02/12/15 Pct Recovery = 35% Analysis Date = 02/12/15 Pct Recovery = 35% Analysis Date = 02/07/15 Pct Recovery = 35% Analysis Date = 02/07/15 Pct Recovery = 35% Analysis Date = 02/02/15 Pct Recovery = 35% Analysis Date = 02/02/15 Pct Recovery = 35% Analysis Date = 01/28/15 Pct Recovery = 35% Analysis Date = 01/28/15 Pct Recovery = 35% Analysis Date = 01/23/15 Pct Recovery = 35% Analysis Date = 01/23/15 Pct Recovery = 35% Analysis Date = 01/18/15 Pct Recovery = 34% Analysis Date = 01/18/15 Pct Recovery = 34% Analysis Date = 01/13/15 Pct Recovery = 34% Analysis Date = 01/13/15 Pct Recovery = 34% Analysis Date = 01/08/15 Pct Recovery = 34% Analysis Date = 01/08/15 Pct Recovery = 34% Analysis Date = 01/03/15 Pct Recovery = 34% Analysis Date = 01/03/15 Pct Recovery = 34% Analysis Date = 12/29/14 Pct Recovery = 34% Analysis Date = 12/29/14 Pct Recovery = 34% Analysis Date = 12/24/14 Pct Recovery = 34% Analysis Date = 12/24/14 Pct Recovery = 34% Analysis Date = 12/19/14 Pct Recovery = 34% Analysis Date = 12/19/14 Pct Recovery = 34% Analysis Date = 12/14/14 Pct Recovery = 34% Analysis Date = 12/14/14 Pct Recovery = 34% Analysis Date = 12/09/14 Pct Recovery = 33% Analysis Date = 12/09/14 Pct Recovery = 33% Analysis Date = 12/04/14 Pct Recovery = 33% Analysis Date = 12/04/14 Pct Recovery = 33% Analysis Date = 11/29/14 Pct Recovery = 33% Analysis Date = 11/29/14 Pct Recovery = 33% Analysis Date = 11/24/14 Pct Recovery = 33% Analysis Date = 11/24/14 Pct Recovery = 33% Analysis Date = 11/19/14 Pct Recovery = 33% Analysis Date = 11/19/14 Pct Recovery = 33% Analysis Date = 11/14/14 Pct Recovery = 33% Analysis Date = 11/14/14 Pct Recovery = 33% Analysis Date = 11/09/14 Pct Recovery = 32% Analysis Date = 11/09/14 Pct Recovery = 32% Analysis Date = 11/04/14 Pct Recovery = 32% Analysis Date = 11/04/14 Pct Recovery = 32% Analysis Date = 10/30/14 Pct Recovery = 32% Analysis Date = 10/30/14 Pct Recovery = 32% Analysis Date = 10/25/14 Pct Recovery = 32% Analysis Date = 10/25/14 Pct Recovery = 32% Analysis Date = 10/20/14 Pct Recovery = 32% Analysis Date = 10/20/14 Pct Recovery = 32% Analysis Date = 10/15/14 Pct Recovery = 31% Analysis Date = 10/15/14 Pct Recovery = 31% Analysis Date = 10/10/14 Pct Recovery = 31% Analysis Date = 10/10/14 Pct Recovery = 31% Analysis Date = 10/05/14 Pct Recovery = 31% Analysis Date = 10/05/14 Pct Recovery = 31% Analysis Date = 09/30/14 Pct Recovery = 31% Analysis Date = 09/30/14 Pct Recovery = 31% Analysis Date = 09/25/14 Pct Recovery = 31% Analysis Date = 09/25/14 Pct Recovery = 31% Analysis Date = 09/20/14 Pct Recovery = 30% Analysis Date = 09/20/14 Pct Recovery = 30% Analysis Date = 09/15/14 Pct Recovery = 30% Analysis Date = 09/15/14 Pct Recovery = 30% Analysis Date = 09/10/14 Pct Recovery = 30% Analysis Date = 09/10/14 Pct Recovery = 30% Analysis Date = 09/05/14 Pct Recovery = 30% Analysis Date = 09/05/14 Pct Recovery = 30% Analysis Date = 08/31/14 Pct Recovery = 30% Analysis Date = 08/31/14 Pct Recovery = 30% Analysis Date = 08/26/14 Pct Recovery = 29% Analysis Date = 08/26/14 Pct Recovery = 29% Analysis Date = 08/21/14 Pct Recovery = 29% Analysis Date = 08/21/14 Pct Recovery = 29% Analysis Date = 08/16/14 Pct Recovery = 29% Analysis Date = 08/16/14 Pct Recovery = 29% Analysis Date = 08/11/14 Pct Recovery = 29% Analysis Date = 08/11/14 Pct Recovery = 29% Analysis Date = 08/06/14 Pct Recovery = 29% Analysis Date = 08/06/14 Pct Recovery = 29% Analysis Date = 08/01/14 Pct Recovery = 29% Analysis Date = 08/01/14 Pct Recovery = 29% Analysis Date = 07/27/14 Pct Recovery = 28% Analysis Date = 07/27/14 Pct Recovery = 28% Analysis Date = 07/22/14 Pct Recovery = 28% Analysis Date = 07/22/14 Pct Recovery = 28% Analysis Date = 07/17/14 Pct Recovery = 28% Analysis Date = 07/17/14 Pct Recovery = 28% Analysis Date = 07/12/14 Pct Recovery = 28% Analysis Date = 07/12/14 Pct Recovery = 28% Analysis Date = 07/07/14 Pct Recovery = 28% Analysis Date = 07/07/14 Pct Recovery = 28% Analysis Date = 07/02/14 Pct Recovery = 27% Analysis Date = 07/02/14 Pct Recovery = 27% Analysis Date = 06/27/14 Pct Recovery = 27% Analysis Date = 06/27/14 Pct Recovery = 27% Analysis Date = 06/22/14 Pct Recovery = 27% Analysis Date = 06/22/14 Pct Recovery = 27% Analysis Date = 06/17/14 Pct Recovery = 27% Analysis Date = 06/17/14 Pct Recovery = 27% Analysis Date = 06/12/14 Pct Recovery = 27% Analysis Date = 06/12/14 Pct Recovery = 27% Analysis Date = 06/07/14 Pct Recovery = 27% Analysis Date = 06/07/14 Pct Recovery = 27% Analysis Date = 06/02/14 Pct Recovery = 27% Analysis Date = 06/02/14 Pct Recovery = 27% Analysis Date = 05/28/14 Pct Recovery = 26% Analysis Date = 05/28/14 Pct Recovery = 26% Analysis Date = 05/23/14 Pct Recovery = 26% Analysis Date = 05/23/14 Pct Recovery = 26% Analysis Date = 05/18/14 Pct Recovery = 26% Analysis Date = 05/18/14 Pct Recovery = 26% Analysis Date = 05/13/14 Pct Recovery = 26% Analysis Date = 05/13/14 Pct Recovery = 26% Analysis Date = 05/08/14 Pct Recovery = 26% Analysis Date = 05/08/14 Pct Recovery = 26% Analysis Date = 05/03/14 Pct Recovery = 26% Analysis Date = 05/03/14 Pct Recovery = 26% Analysis Date = 04/28/14 Pct Recovery = 26% Analysis Date = 04/28/14 Pct Recovery = 26% Analysis Date = 04/23/14 Pct Recovery = 25% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
RANITIDINE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 44 34% 18% 39% 20%
Total 44 34% 18% 39% 20%

Sample Statistics
RANITIDINE

Characteristic N % % Basis
Plotted 44 64% Spiked
Estimated Values 44 64% Spiked
Deleted Values 9 8% Spiked + Not Spiked
Spiked, Censored 2 3% Spiked
Spiked 76 .  
False Negatives 23 33% 23 out of 69
Not Spiked 39 .  
False Positives 0 0% 0 out of 37

BQS OBSP Determination:
SERTRALINE
METHOD: 2440 , TESTIDCODE: 67528LCM56
Open Data Set

Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 44% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 41% Analysis Date = 11/24/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 60% Analysis Date = 10/01/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 56% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 80 µl & ERA 0406-15-08: 80 µl Pct Recovery = 54% Analysis Date = 11/05/15 SpikeMix = ERA 0406-15-08: 80 µl & Abs 052215: 80 µl Pct Recovery = 55% Analysis Date = 09/24/16 SpikeMix = Crescent EN160610015: 80 µl & Abs 061416: 80 µl Pct Recovery = 32% Analysis Date = 09/24/16 SpikeMix = Abs 061416: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 38% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 49% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 45% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 39% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 45% Analysis Date = 11/18/16 SpikeMix = ERA 04281604: 80 µl & ERA 04281603: 80 µl Pct Recovery = 40% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & ERA 04281604: 80 µl Pct Recovery = 30% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-04: 15 µl & Abs 041814: 15 µl Pct Recovery = 36% Analysis Date = 02/06/15 SpikeMix = Abs 041814: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 44% Analysis Date = 07/12/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 52% Analysis Date = 06/22/14 SpikeMix = Abs 041814: 60 µl & Abs 041614: 60 µl Pct Recovery = 72% Analysis Date = 05/21/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 51% Analysis Date = 05/07/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 39% Analysis Date = 04/29/15 SpikeMix = ERA 0319-14-05: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 63% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 44% Analysis Date = 01/16/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 49% Analysis Date = 12/07/14 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 46% Analysis Date = 12/06/14 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 39% Analysis Date = 08/28/14 SpikeMix = ERA 0319-14-04: 60 µl & ERA 0319-14-05: 60 µl Pct Recovery = 49% Analysis Date = 07/26/14 SpikeMix = ERA 0319-14-05: 60 µl & ERA 0318-14-02: 60 µl Pct Recovery = 60% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 60% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 55% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-07A: 40 µl & Abs 051315: 40 µl Pct Recovery = 47% Analysis Date = 07/31/15 SpikeMix = Abs 051315: 40 µl & Abs 052215: 40 µl Pct Recovery = 46% Analysis Date = 07/30/15 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 55% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-08: 40 µl & Abs 052215: 40 µl Pct Recovery = 59% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 40% Analysis Date = 11/04/15 SpikeMix = ERA 0406-15-07A: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 49% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-08: 40 µl & ERA 0406-15-09: 40 µl Pct Recovery = 40% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 40% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 43% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 24% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 32% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 29% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 27% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 13% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 24% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 53% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 61% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 53% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 52% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 24% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 37% Analysis Date = 04/10/15 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 40% Analysis Date = 11/04/14 SpikeMix = Abs 041814: 8 µl & ERA 0318-14-02: 8 µl Pct Recovery = 21% Analysis Date = 10/11/14 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 30% Analysis Date = 11/04/14 SpikeMix = Abs 041714: 8 µl & ERA 0319-14-05: 8 µl Pct Recovery = 22% Analysis Date = 10/24/14 SpikeMix = ERA 0319-14-05: 8 µl & Abs 041614: 8 µl Pct Recovery = 48% Analysis Date = 10/10/14 SpikeMix = Abs 041714: 30 µl & Abs 041814: 30 µl Pct Recovery = 50% Analysis Date = 10/10/14 SpikeMix = Abs 041814: 30 µl & ERA 0318-14-02: 30 µl Pct Recovery = 41% Analysis Date = 07/13/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 49% Analysis Date = 05/30/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 48% Analysis Date = 08/30/14 SpikeMix = ERA 0318-14-02: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 50% Analysis Date = 08/16/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 20% Analysis Date = 02/23/16 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 49% Analysis Date = 06/26/15 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 34% Analysis Date = 04/27/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 65% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 37% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-08: 20 µl & ERA 0406-15-09: 20 µl Pct Recovery = 36% Analysis Date = 09/15/15 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 56% Analysis Date = 01/04/17 Pct Recovery = 39% Analysis Date = 12/31/16 Pct Recovery = 39% Analysis Date = 12/31/16 Pct Recovery = 39% Analysis Date = 12/26/16 Pct Recovery = 39% Analysis Date = 12/26/16 Pct Recovery = 39% Analysis Date = 12/21/16 Pct Recovery = 39% Analysis Date = 12/21/16 Pct Recovery = 39% Analysis Date = 12/16/16 Pct Recovery = 39% Analysis Date = 12/16/16 Pct Recovery = 39% Analysis Date = 12/11/16 Pct Recovery = 39% Analysis Date = 12/11/16 Pct Recovery = 39% Analysis Date = 12/07/16 Pct Recovery = 39% Analysis Date = 12/07/16 Pct Recovery = 39% Analysis Date = 12/02/16 Pct Recovery = 39% Analysis Date = 12/02/16 Pct Recovery = 39% Analysis Date = 11/27/16 Pct Recovery = 39% Analysis Date = 11/27/16 Pct Recovery = 39% Analysis Date = 11/22/16 Pct Recovery = 39% Analysis Date = 11/22/16 Pct Recovery = 39% Analysis Date = 11/17/16 Pct Recovery = 39% Analysis Date = 11/17/16 Pct Recovery = 39% Analysis Date = 11/13/16 Pct Recovery = 39% Analysis Date = 11/13/16 Pct Recovery = 39% Analysis Date = 11/08/16 Pct Recovery = 39% Analysis Date = 11/08/16 Pct Recovery = 39% Analysis Date = 11/03/16 Pct Recovery = 39% Analysis Date = 11/03/16 Pct Recovery = 39% Analysis Date = 10/29/16 Pct Recovery = 39% Analysis Date = 10/29/16 Pct Recovery = 39% Analysis Date = 10/24/16 Pct Recovery = 39% Analysis Date = 10/24/16 Pct Recovery = 39% Analysis Date = 10/20/16 Pct Recovery = 40% Analysis Date = 10/20/16 Pct Recovery = 40% Analysis Date = 10/15/16 Pct Recovery = 40% Analysis Date = 10/15/16 Pct Recovery = 40% Analysis Date = 10/10/16 Pct Recovery = 40% Analysis Date = 10/10/16 Pct Recovery = 40% Analysis Date = 10/05/16 Pct Recovery = 40% Analysis Date = 10/05/16 Pct Recovery = 40% Analysis Date = 09/30/16 Pct Recovery = 40% Analysis Date = 09/30/16 Pct Recovery = 40% Analysis Date = 09/26/16 Pct Recovery = 40% Analysis Date = 09/26/16 Pct Recovery = 40% Analysis Date = 09/21/16 Pct Recovery = 40% Analysis Date = 09/21/16 Pct Recovery = 40% Analysis Date = 09/16/16 Pct Recovery = 40% Analysis Date = 09/16/16 Pct Recovery = 40% Analysis Date = 09/11/16 Pct Recovery = 40% Analysis Date = 09/11/16 Pct Recovery = 40% Analysis Date = 09/06/16 Pct Recovery = 40% Analysis Date = 09/06/16 Pct Recovery = 40% Analysis Date = 09/02/16 Pct Recovery = 41% Analysis Date = 09/02/16 Pct Recovery = 41% Analysis Date = 08/28/16 Pct Recovery = 41% Analysis Date = 08/28/16 Pct Recovery = 41% Analysis Date = 08/23/16 Pct Recovery = 41% Analysis Date = 08/23/16 Pct Recovery = 41% Analysis Date = 08/18/16 Pct Recovery = 41% Analysis Date = 08/18/16 Pct Recovery = 41% Analysis Date = 08/13/16 Pct Recovery = 41% Analysis Date = 08/13/16 Pct Recovery = 41% Analysis Date = 08/09/16 Pct Recovery = 41% Analysis Date = 08/09/16 Pct Recovery = 41% Analysis Date = 08/04/16 Pct Recovery = 41% Analysis Date = 08/04/16 Pct Recovery = 41% Analysis Date = 07/30/16 Pct Recovery = 41% Analysis Date = 07/30/16 Pct Recovery = 41% Analysis Date = 07/25/16 Pct Recovery = 42% Analysis Date = 07/25/16 Pct Recovery = 42% Analysis Date = 07/20/16 Pct Recovery = 42% Analysis Date = 07/20/16 Pct Recovery = 42% Analysis Date = 07/16/16 Pct Recovery = 42% Analysis Date = 07/16/16 Pct Recovery = 42% Analysis Date = 07/11/16 Pct Recovery = 42% Analysis Date = 07/11/16 Pct Recovery = 42% Analysis Date = 07/06/16 Pct Recovery = 42% Analysis Date = 07/06/16 Pct Recovery = 42% Analysis Date = 07/01/16 Pct Recovery = 42% Analysis Date = 07/01/16 Pct Recovery = 42% Analysis Date = 06/26/16 Pct Recovery = 43% Analysis Date = 06/26/16 Pct Recovery = 43% Analysis Date = 06/22/16 Pct Recovery = 43% Analysis Date = 06/22/16 Pct Recovery = 43% Analysis Date = 06/17/16 Pct Recovery = 43% Analysis Date = 06/17/16 Pct Recovery = 43% Analysis Date = 06/12/16 Pct Recovery = 43% Analysis Date = 06/12/16 Pct Recovery = 43% Analysis Date = 06/07/16 Pct Recovery = 43% Analysis Date = 06/07/16 Pct Recovery = 43% Analysis Date = 06/02/16 Pct Recovery = 43% Analysis Date = 06/02/16 Pct Recovery = 43% Analysis Date = 05/29/16 Pct Recovery = 44% Analysis Date = 05/29/16 Pct Recovery = 44% Analysis Date = 05/24/16 Pct Recovery = 44% Analysis Date = 05/24/16 Pct Recovery = 44% Analysis Date = 05/19/16 Pct Recovery = 44% Analysis Date = 05/19/16 Pct Recovery = 44% Analysis Date = 05/14/16 Pct Recovery = 44% Analysis Date = 05/14/16 Pct Recovery = 44% Analysis Date = 05/09/16 Pct Recovery = 44% Analysis Date = 05/09/16 Pct Recovery = 44% Analysis Date = 05/05/16 Pct Recovery = 45% Analysis Date = 05/05/16 Pct Recovery = 45% Analysis Date = 04/30/16 Pct Recovery = 45% Analysis Date = 04/30/16 Pct Recovery = 45% Analysis Date = 04/25/16 Pct Recovery = 45% Analysis Date = 04/25/16 Pct Recovery = 45% Analysis Date = 04/20/16 Pct Recovery = 45% Analysis Date = 04/20/16 Pct Recovery = 45% Analysis Date = 04/15/16 Pct Recovery = 45% Analysis Date = 04/15/16 Pct Recovery = 45% Analysis Date = 04/11/16 Pct Recovery = 45% Analysis Date = 04/11/16 Pct Recovery = 45% Analysis Date = 04/06/16 Pct Recovery = 46% Analysis Date = 04/06/16 Pct Recovery = 46% Analysis Date = 04/01/16 Pct Recovery = 46% Analysis Date = 04/01/16 Pct Recovery = 46% Analysis Date = 03/27/16 Pct Recovery = 46% Analysis Date = 03/27/16 Pct Recovery = 46% Analysis Date = 03/22/16 Pct Recovery = 46% Analysis Date = 03/22/16 Pct Recovery = 46% Analysis Date = 03/18/16 Pct Recovery = 46% Analysis Date = 03/18/16 Pct Recovery = 46% Analysis Date = 03/13/16 Pct Recovery = 46% Analysis Date = 03/13/16 Pct Recovery = 46% Analysis Date = 03/08/16 Pct Recovery = 47% Analysis Date = 03/08/16 Pct Recovery = 47% Analysis Date = 03/03/16 Pct Recovery = 47% Analysis Date = 03/03/16 Pct Recovery = 47% Analysis Date = 02/27/16 Pct Recovery = 47% Analysis Date = 02/27/16 Pct Recovery = 47% Analysis Date = 02/23/16 Pct Recovery = 47% Analysis Date = 02/23/16 Pct Recovery = 47% Analysis Date = 02/18/16 Pct Recovery = 47% Analysis Date = 02/18/16 Pct Recovery = 47% Analysis Date = 02/13/16 Pct Recovery = 47% Analysis Date = 02/13/16 Pct Recovery = 47% Analysis Date = 02/08/16 Pct Recovery = 47% Analysis Date = 02/08/16 Pct Recovery = 47% Analysis Date = 02/03/16 Pct Recovery = 48% Analysis Date = 02/03/16 Pct Recovery = 48% Analysis Date = 01/30/16 Pct Recovery = 48% Analysis Date = 01/30/16 Pct Recovery = 48% Analysis Date = 01/25/16 Pct Recovery = 48% Analysis Date = 01/25/16 Pct Recovery = 48% Analysis Date = 01/20/16 Pct Recovery = 48% Analysis Date = 01/20/16 Pct Recovery = 48% Analysis Date = 01/15/16 Pct Recovery = 48% Analysis Date = 01/15/16 Pct Recovery = 48% Analysis Date = 01/10/16 Pct Recovery = 48% Analysis Date = 01/10/16 Pct Recovery = 48% Analysis Date = 01/06/16 Pct Recovery = 48% Analysis Date = 01/06/16 Pct Recovery = 48% Analysis Date = 01/01/16 Pct Recovery = 48% Analysis Date = 01/01/16 Pct Recovery = 48% Analysis Date = 12/27/15 Pct Recovery = 48% Analysis Date = 12/27/15 Pct Recovery = 48% Analysis Date = 12/22/15 Pct Recovery = 49% Analysis Date = 12/22/15 Pct Recovery = 49% Analysis Date = 12/17/15 Pct Recovery = 49% Analysis Date = 12/17/15 Pct Recovery = 49% Analysis Date = 12/13/15 Pct Recovery = 49% Analysis Date = 12/13/15 Pct Recovery = 49% Analysis Date = 12/08/15 Pct Recovery = 49% Analysis Date = 12/08/15 Pct Recovery = 49% Analysis Date = 12/03/15 Pct Recovery = 49% Analysis Date = 12/03/15 Pct Recovery = 49% Analysis Date = 11/28/15 Pct Recovery = 49% Analysis Date = 11/28/15 Pct Recovery = 49% Analysis Date = 11/23/15 Pct Recovery = 49% Analysis Date = 11/23/15 Pct Recovery = 49% Analysis Date = 11/19/15 Pct Recovery = 48% Analysis Date = 11/19/15 Pct Recovery = 48% Analysis Date = 11/14/15 Pct Recovery = 48% Analysis Date = 11/14/15 Pct Recovery = 48% Analysis Date = 11/09/15 Pct Recovery = 48% Analysis Date = 11/09/15 Pct Recovery = 48% Analysis Date = 11/04/15 Pct Recovery = 48% Analysis Date = 11/04/15 Pct Recovery = 48% Analysis Date = 10/30/15 Pct Recovery = 48% Analysis Date = 10/30/15 Pct Recovery = 48% Analysis Date = 10/26/15 Pct Recovery = 48% Analysis Date = 10/26/15 Pct Recovery = 48% Analysis Date = 10/21/15 Pct Recovery = 48% Analysis Date = 10/21/15 Pct Recovery = 48% Analysis Date = 10/16/15 Pct Recovery = 48% Analysis Date = 10/16/15 Pct Recovery = 48% Analysis Date = 10/11/15 Pct Recovery = 48% Analysis Date = 10/11/15 Pct Recovery = 48% Analysis Date = 10/06/15 Pct Recovery = 48% Analysis Date = 10/06/15 Pct Recovery = 48% Analysis Date = 10/02/15 Pct Recovery = 48% Analysis Date = 10/02/15 Pct Recovery = 48% Analysis Date = 09/27/15 Pct Recovery = 48% Analysis Date = 09/27/15 Pct Recovery = 48% Analysis Date = 09/22/15 Pct Recovery = 48% Analysis Date = 09/22/15 Pct Recovery = 48% Analysis Date = 09/17/15 Pct Recovery = 48% Analysis Date = 09/17/15 Pct Recovery = 48% Analysis Date = 09/12/15 Pct Recovery = 48% Analysis Date = 09/12/15 Pct Recovery = 48% Analysis Date = 09/08/15 Pct Recovery = 47% Analysis Date = 09/08/15 Pct Recovery = 47% Analysis Date = 09/03/15 Pct Recovery = 47% Analysis Date = 09/03/15 Pct Recovery = 47% Analysis Date = 08/29/15 Pct Recovery = 47% Analysis Date = 08/29/15 Pct Recovery = 47% Analysis Date = 08/24/15 Pct Recovery = 47% Analysis Date = 08/24/15 Pct Recovery = 47% Analysis Date = 08/19/15 Pct Recovery = 47% Analysis Date = 08/19/15 Pct Recovery = 47% Analysis Date = 08/15/15 Pct Recovery = 47% Analysis Date = 08/15/15 Pct Recovery = 47% Analysis Date = 08/10/15 Pct Recovery = 47% Analysis Date = 08/10/15 Pct Recovery = 47% Analysis Date = 08/05/15 Pct Recovery = 47% Analysis Date = 08/05/15 Pct Recovery = 47% Analysis Date = 07/31/15 Pct Recovery = 47% Analysis Date = 07/31/15 Pct Recovery = 47% Analysis Date = 07/26/15 Pct Recovery = 47% Analysis Date = 07/26/15 Pct Recovery = 47% Analysis Date = 07/22/15 Pct Recovery = 47% Analysis Date = 07/22/15 Pct Recovery = 47% Analysis Date = 07/17/15 Pct Recovery = 47% Analysis Date = 07/17/15 Pct Recovery = 47% Analysis Date = 07/12/15 Pct Recovery = 47% Analysis Date = 07/12/15 Pct Recovery = 47% Analysis Date = 07/07/15 Pct Recovery = 46% Analysis Date = 07/07/15 Pct Recovery = 46% Analysis Date = 07/02/15 Pct Recovery = 46% Analysis Date = 07/02/15 Pct Recovery = 46% Analysis Date = 06/28/15 Pct Recovery = 46% Analysis Date = 06/28/15 Pct Recovery = 46% Analysis Date = 06/23/15 Pct Recovery = 46% Analysis Date = 06/23/15 Pct Recovery = 46% Analysis Date = 06/18/15 Pct Recovery = 46% Analysis Date = 06/18/15 Pct Recovery = 46% Analysis Date = 06/13/15 Pct Recovery = 46% Analysis Date = 06/13/15 Pct Recovery = 46% Analysis Date = 06/08/15 Pct Recovery = 46% Analysis Date = 06/08/15 Pct Recovery = 46% Analysis Date = 06/04/15 Pct Recovery = 46% Analysis Date = 06/04/15 Pct Recovery = 46% Analysis Date = 05/30/15 Pct Recovery = 46% Analysis Date = 05/30/15 Pct Recovery = 46% Analysis Date = 05/25/15 Pct Recovery = 46% Analysis Date = 05/25/15 Pct Recovery = 46% Analysis Date = 05/20/15 Pct Recovery = 45% Analysis Date = 05/20/15 Pct Recovery = 45% Analysis Date = 05/15/15 Pct Recovery = 45% Analysis Date = 05/15/15 Pct Recovery = 45% Analysis Date = 05/11/15 Pct Recovery = 45% Analysis Date = 05/11/15 Pct Recovery = 45% Analysis Date = 05/06/15 Pct Recovery = 45% Analysis Date = 05/06/15 Pct Recovery = 45% Analysis Date = 05/01/15 Pct Recovery = 45% Analysis Date = 05/01/15 Pct Recovery = 45% Analysis Date = 04/26/15 Pct Recovery = 45% Analysis Date = 04/26/15 Pct Recovery = 45% Analysis Date = 04/21/15 Pct Recovery = 45% Analysis Date = 04/21/15 Pct Recovery = 45% Analysis Date = 04/17/15 Pct Recovery = 45% Analysis Date = 04/17/15 Pct Recovery = 45% Analysis Date = 04/12/15 Pct Recovery = 45% Analysis Date = 04/12/15 Pct Recovery = 45% Analysis Date = 04/07/15 Pct Recovery = 45% Analysis Date = 04/07/15 Pct Recovery = 45% Analysis Date = 04/02/15 Pct Recovery = 45% Analysis Date = 04/02/15 Pct Recovery = 45% Analysis Date = 03/28/15 Pct Recovery = 45% Analysis Date = 03/28/15 Pct Recovery = 45% Analysis Date = 03/24/15 Pct Recovery = 45% Analysis Date = 03/24/15 Pct Recovery = 45% Analysis Date = 03/19/15 Pct Recovery = 45% Analysis Date = 03/19/15 Pct Recovery = 45% Analysis Date = 03/14/15 Pct Recovery = 45% Analysis Date = 03/14/15 Pct Recovery = 45% Analysis Date = 03/09/15 Pct Recovery = 45% Analysis Date = 03/09/15 Pct Recovery = 45% Analysis Date = 03/04/15 Pct Recovery = 45% Analysis Date = 03/04/15 Pct Recovery = 45% Analysis Date = 02/28/15 Pct Recovery = 45% Analysis Date = 02/28/15 Pct Recovery = 45% Analysis Date = 02/23/15 Pct Recovery = 45% Analysis Date = 02/23/15 Pct Recovery = 45% Analysis Date = 02/18/15 Pct Recovery = 45% Analysis Date = 02/18/15 Pct Recovery = 45% Analysis Date = 02/13/15 Pct Recovery = 45% Analysis Date = 02/13/15 Pct Recovery = 45% Analysis Date = 02/08/15 Pct Recovery = 45% Analysis Date = 02/08/15 Pct Recovery = 45% Analysis Date = 02/04/15 Pct Recovery = 45% Analysis Date = 02/04/15 Pct Recovery = 45% Analysis Date = 01/30/15 Pct Recovery = 45% Analysis Date = 01/30/15 Pct Recovery = 45% Analysis Date = 01/25/15 Pct Recovery = 45% Analysis Date = 01/25/15 Pct Recovery = 45% Analysis Date = 01/20/15 Pct Recovery = 45% Analysis Date = 01/20/15 Pct Recovery = 45% Analysis Date = 01/15/15 Pct Recovery = 45% Analysis Date = 01/15/15 Pct Recovery = 45% Analysis Date = 01/11/15 Pct Recovery = 45% Analysis Date = 01/11/15 Pct Recovery = 45% Analysis Date = 01/06/15 Pct Recovery = 45% Analysis Date = 01/06/15 Pct Recovery = 45% Analysis Date = 01/01/15 Pct Recovery = 45% Analysis Date = 01/01/15 Pct Recovery = 45% Analysis Date = 12/27/14 Pct Recovery = 45% Analysis Date = 12/27/14 Pct Recovery = 45% Analysis Date = 12/22/14 Pct Recovery = 45% Analysis Date = 12/22/14 Pct Recovery = 45% Analysis Date = 12/18/14 Pct Recovery = 45% Analysis Date = 12/18/14 Pct Recovery = 45% Analysis Date = 12/13/14 Pct Recovery = 45% Analysis Date = 12/13/14 Pct Recovery = 45% Analysis Date = 12/08/14 Pct Recovery = 45% Analysis Date = 12/08/14 Pct Recovery = 45% Analysis Date = 12/03/14 Pct Recovery = 45% Analysis Date = 12/03/14 Pct Recovery = 45% Analysis Date = 11/28/14 Pct Recovery = 45% Analysis Date = 11/28/14 Pct Recovery = 45% Analysis Date = 11/24/14 Pct Recovery = 45% Analysis Date = 11/24/14 Pct Recovery = 45% Analysis Date = 11/19/14 Pct Recovery = 45% Analysis Date = 11/19/14 Pct Recovery = 45% Analysis Date = 11/14/14 Pct Recovery = 45% Analysis Date = 11/14/14 Pct Recovery = 45% Analysis Date = 11/09/14 Pct Recovery = 45% Analysis Date = 11/09/14 Pct Recovery = 45% Analysis Date = 11/04/14 Pct Recovery = 45% Analysis Date = 11/04/14 Pct Recovery = 45% Analysis Date = 10/31/14 Pct Recovery = 45% Analysis Date = 10/31/14 Pct Recovery = 45% Analysis Date = 10/26/14 Pct Recovery = 45% Analysis Date = 10/26/14 Pct Recovery = 45% Analysis Date = 10/21/14 Pct Recovery = 45% Analysis Date = 10/21/14 Pct Recovery = 45% Analysis Date = 10/16/14 Pct Recovery = 45% Analysis Date = 10/16/14 Pct Recovery = 45% Analysis Date = 10/11/14 Pct Recovery = 45% Analysis Date = 10/11/14 Pct Recovery = 45% Analysis Date = 10/07/14 Pct Recovery = 45% Analysis Date = 10/07/14 Pct Recovery = 45% Analysis Date = 10/02/14 Pct Recovery = 45% Analysis Date = 10/02/14 Pct Recovery = 45% Analysis Date = 09/27/14 Pct Recovery = 45% Analysis Date = 09/27/14 Pct Recovery = 45% Analysis Date = 09/22/14 Pct Recovery = 45% Analysis Date = 09/22/14 Pct Recovery = 45% Analysis Date = 09/17/14 Pct Recovery = 45% Analysis Date = 09/17/14 Pct Recovery = 45% Analysis Date = 09/13/14 Pct Recovery = 45% Analysis Date = 09/13/14 Pct Recovery = 45% Analysis Date = 09/08/14 Pct Recovery = 45% Analysis Date = 09/08/14 Pct Recovery = 45% Analysis Date = 09/03/14 Pct Recovery = 45% Analysis Date = 09/03/14 Pct Recovery = 45% Analysis Date = 08/29/14 Pct Recovery = 45% Analysis Date = 08/29/14 Pct Recovery = 45% Analysis Date = 08/24/14 Pct Recovery = 45% Analysis Date = 08/24/14 Pct Recovery = 45% Analysis Date = 08/20/14 Pct Recovery = 45% Analysis Date = 08/20/14 Pct Recovery = 45% Analysis Date = 08/15/14 Pct Recovery = 45% Analysis Date = 08/15/14 Pct Recovery = 45% Analysis Date = 08/10/14 Pct Recovery = 45% Analysis Date = 08/10/14 Pct Recovery = 45% Analysis Date = 08/05/14 Pct Recovery = 45% Analysis Date = 08/05/14 Pct Recovery = 45% Analysis Date = 07/31/14 Pct Recovery = 45% Analysis Date = 07/31/14 Pct Recovery = 45% Analysis Date = 07/27/14 Pct Recovery = 45% Analysis Date = 07/27/14 Pct Recovery = 45% Analysis Date = 07/22/14 Pct Recovery = 45% Analysis Date = 07/22/14 Pct Recovery = 45% Analysis Date = 07/17/14 Pct Recovery = 45% Analysis Date = 07/17/14 Pct Recovery = 45% Analysis Date = 07/12/14 Pct Recovery = 45% Analysis Date = 07/12/14 Pct Recovery = 45% Analysis Date = 07/07/14 Pct Recovery = 46% Analysis Date = 07/07/14 Pct Recovery = 46% Analysis Date = 07/03/14 Pct Recovery = 46% Analysis Date = 07/03/14 Pct Recovery = 46% Analysis Date = 06/28/14 Pct Recovery = 46% Analysis Date = 06/28/14 Pct Recovery = 46% Analysis Date = 06/23/14 Pct Recovery = 46% Analysis Date = 06/23/14 Pct Recovery = 46% Analysis Date = 06/18/14 Pct Recovery = 46% Analysis Date = 06/18/14 Pct Recovery = 46% Analysis Date = 06/13/14 Pct Recovery = 46% Analysis Date = 06/13/14 Pct Recovery = 46% Analysis Date = 06/09/14 Pct Recovery = 46% Analysis Date = 06/09/14 Pct Recovery = 46% Analysis Date = 06/04/14 Pct Recovery = 46% Analysis Date = 06/04/14 Pct Recovery = 46% Analysis Date = 05/30/14 Pct Recovery = 46% Analysis Date = 05/30/14 Pct Recovery = 46% Analysis Date = 05/25/14 Pct Recovery = 46% Analysis Date = 05/25/14 Pct Recovery = 46% Analysis Date = 05/21/14 Pct Recovery = 46% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
SERTRALINE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 67 44% 12% 45% 11%
Total 67 44% 12% 45% 11%

Sample Statistics
SERTRALINE

Characteristic N % % Basis
Plotted 67 89% Spiked
Estimated Values 67 89% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 2 3% Spiked
Spiked 75 .  
False Negatives 6 8% 6 out of 75
Not Spiked 40 .  
False Positives 0 0% 0 out of 40

BQS OBSP Determination:
SITAGLIPTIN
METHOD: 2440 , TESTIDCODE: 67531LCM56
Open Data Set

Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 89% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 82% Analysis Date = 11/24/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 74% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 80 µl & Abs 051315: 80 µl Pct Recovery = 69% Analysis Date = 10/01/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 19% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 83% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 82% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 76% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 82% Analysis Date = 11/18/16 SpikeMix = ERA 04281604: 80 µl & ERA 04281603: 80 µl Pct Recovery = 70% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & ERA 04281604: 80 µl Pct Recovery = 75% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 65% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 67% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 70% Analysis Date = 12/07/14 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 80% Analysis Date = 10/25/14 SpikeMix = Abs 041614: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 86% Analysis Date = 06/22/14 SpikeMix = Abs 041814: 60 µl & Abs 041614: 60 µl Pct Recovery = 79% Analysis Date = 06/11/14 SpikeMix = Abs 041614: 60 µl & Abs 041714: 60 µl Pct Recovery = 50% Analysis Date = 04/29/15 SpikeMix = ERA 0319-14-05: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 117% Analysis Date = 03/11/15 SpikeMix = ERA 0318-14-02: 15 µl & Abs 041714: 15 µl Pct Recovery = 113% Analysis Date = 02/06/15 SpikeMix = Abs 041814: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 99% Analysis Date = 12/06/14 SpikeMix = ERA 0318-14-02: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 82% Analysis Date = 10/11/14 SpikeMix = ERA 0318-14-02: 60 µl & ERA 0319-14-04: 60 µl Pct Recovery = 84% Analysis Date = 08/21/14 SpikeMix = ERA 0318-14-02: 60 µl & Abs 041714: 60 µl Pct Recovery = 54% Analysis Date = 07/26/14 SpikeMix = ERA 0319-14-05: 60 µl & ERA 0318-14-02: 60 µl Pct Recovery = 69% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 61% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 58% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-07A: 40 µl & Abs 051315: 40 µl Pct Recovery = 69% Analysis Date = 07/31/15 SpikeMix = Abs 051315: 40 µl & Abs 052215: 40 µl Pct Recovery = 54% Analysis Date = 07/30/15 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 66% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 121% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 137% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 83% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 73% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 84% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 99% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 63% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 70% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 74% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 82% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 65% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 82% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 63% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 68% Analysis Date = 04/30/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 86% Analysis Date = 02/10/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 76% Analysis Date = 10/24/14 SpikeMix = ERA 0319-14-05: 8 µl & Abs 041614: 8 µl Pct Recovery = 75% Analysis Date = 12/07/14 SpikeMix = ERA 0318-14-02: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 98% Analysis Date = 11/04/14 SpikeMix = Abs 041814: 8 µl & ERA 0318-14-02: 8 µl Pct Recovery = 98% Analysis Date = 09/12/14 SpikeMix = Abs 041614: 30 µl & ERA 0319-14-04: 30 µl Pct Recovery = 62% Analysis Date = 07/13/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 44% Analysis Date = 06/28/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 45% Analysis Date = 05/30/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 42% Analysis Date = 05/17/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 54% Analysis Date = 10/10/14 SpikeMix = Abs 041814: 30 µl & ERA 0318-14-02: 30 µl Pct Recovery = 99% Analysis Date = 08/30/14 SpikeMix = ERA 0318-14-02: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 76% Analysis Date = 07/20/14 SpikeMix = ERA 0318-14-02: 30 µl & Abs 041714: 30 µl Pct Recovery = 49% Analysis Date = 02/23/16 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 50% Analysis Date = 08/11/15 SpikeMix = Abs 050115: 20 µl & Abs 051315: 20 µl Pct Recovery = 55% Analysis Date = 06/26/15 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 55% Analysis Date = 06/09/15 SpikeMix = Abs 051315: 20 µl & Abs 050115: 20 µl Pct Recovery = 55% Analysis Date = 04/09/16 SpikeMix = Abs 051315: 10 µl & ERA 0406-15-09: 10 µl Pct Recovery = 80% Analysis Date = 04/09/16 SpikeMix = Abs 051315: 10 µl & ERA 0406-15-09: 10 µl Pct Recovery = 128% Analysis Date = 01/18/17 Pct Recovery = 88% Analysis Date = 01/14/17 Pct Recovery = 88% Analysis Date = 01/14/17 Pct Recovery = 88% Analysis Date = 01/09/17 Pct Recovery = 87% Analysis Date = 01/09/17 Pct Recovery = 87% Analysis Date = 01/04/17 Pct Recovery = 87% Analysis Date = 01/04/17 Pct Recovery = 87% Analysis Date = 12/30/16 Pct Recovery = 87% Analysis Date = 12/30/16 Pct Recovery = 87% Analysis Date = 12/25/16 Pct Recovery = 86% Analysis Date = 12/25/16 Pct Recovery = 86% Analysis Date = 12/20/16 Pct Recovery = 86% Analysis Date = 12/20/16 Pct Recovery = 86% Analysis Date = 12/15/16 Pct Recovery = 86% Analysis Date = 12/15/16 Pct Recovery = 86% Analysis Date = 12/10/16 Pct Recovery = 85% Analysis Date = 12/10/16 Pct Recovery = 85% Analysis Date = 12/05/16 Pct Recovery = 85% Analysis Date = 12/05/16 Pct Recovery = 85% Analysis Date = 12/01/16 Pct Recovery = 85% Analysis Date = 12/01/16 Pct Recovery = 85% Analysis Date = 11/26/16 Pct Recovery = 84% Analysis Date = 11/26/16 Pct Recovery = 84% Analysis Date = 11/21/16 Pct Recovery = 84% Analysis Date = 11/21/16 Pct Recovery = 84% Analysis Date = 11/16/16 Pct Recovery = 84% Analysis Date = 11/16/16 Pct Recovery = 84% Analysis Date = 11/11/16 Pct Recovery = 84% Analysis Date = 11/11/16 Pct Recovery = 84% Analysis Date = 11/06/16 Pct Recovery = 83% Analysis Date = 11/06/16 Pct Recovery = 83% Analysis Date = 11/01/16 Pct Recovery = 83% Analysis Date = 11/01/16 Pct Recovery = 83% Analysis Date = 10/27/16 Pct Recovery = 83% Analysis Date = 10/27/16 Pct Recovery = 83% Analysis Date = 10/22/16 Pct Recovery = 82% Analysis Date = 10/22/16 Pct Recovery = 82% Analysis Date = 10/18/16 Pct Recovery = 82% Analysis Date = 10/18/16 Pct Recovery = 82% Analysis Date = 10/13/16 Pct Recovery = 82% Analysis Date = 10/13/16 Pct Recovery = 82% Analysis Date = 10/08/16 Pct Recovery = 81% Analysis Date = 10/08/16 Pct Recovery = 81% Analysis Date = 10/03/16 Pct Recovery = 81% Analysis Date = 10/03/16 Pct Recovery = 81% Analysis Date = 09/28/16 Pct Recovery = 81% Analysis Date = 09/28/16 Pct Recovery = 81% Analysis Date = 09/23/16 Pct Recovery = 80% Analysis Date = 09/23/16 Pct Recovery = 80% Analysis Date = 09/18/16 Pct Recovery = 80% Analysis Date = 09/18/16 Pct Recovery = 80% Analysis Date = 09/13/16 Pct Recovery = 80% Analysis Date = 09/13/16 Pct Recovery = 80% Analysis Date = 09/08/16 Pct Recovery = 80% Analysis Date = 09/08/16 Pct Recovery = 80% Analysis Date = 09/04/16 Pct Recovery = 79% Analysis Date = 09/04/16 Pct Recovery = 79% Analysis Date = 08/30/16 Pct Recovery = 79% Analysis Date = 08/30/16 Pct Recovery = 79% Analysis Date = 08/25/16 Pct Recovery = 79% Analysis Date = 08/25/16 Pct Recovery = 79% Analysis Date = 08/20/16 Pct Recovery = 78% Analysis Date = 08/20/16 Pct Recovery = 78% Analysis Date = 08/15/16 Pct Recovery = 78% Analysis Date = 08/15/16 Pct Recovery = 78% Analysis Date = 08/10/16 Pct Recovery = 78% Analysis Date = 08/10/16 Pct Recovery = 78% Analysis Date = 08/05/16 Pct Recovery = 77% Analysis Date = 08/05/16 Pct Recovery = 77% Analysis Date = 07/31/16 Pct Recovery = 77% Analysis Date = 07/31/16 Pct Recovery = 77% Analysis Date = 07/26/16 Pct Recovery = 77% Analysis Date = 07/26/16 Pct Recovery = 77% Analysis Date = 07/22/16 Pct Recovery = 77% Analysis Date = 07/22/16 Pct Recovery = 77% Analysis Date = 07/17/16 Pct Recovery = 76% Analysis Date = 07/17/16 Pct Recovery = 76% Analysis Date = 07/12/16 Pct Recovery = 76% Analysis Date = 07/12/16 Pct Recovery = 76% Analysis Date = 07/07/16 Pct Recovery = 76% Analysis Date = 07/07/16 Pct Recovery = 76% Analysis Date = 07/02/16 Pct Recovery = 76% Analysis Date = 07/02/16 Pct Recovery = 76% Analysis Date = 06/27/16 Pct Recovery = 75% Analysis Date = 06/27/16 Pct Recovery = 75% Analysis Date = 06/22/16 Pct Recovery = 75% Analysis Date = 06/22/16 Pct Recovery = 75% Analysis Date = 06/17/16 Pct Recovery = 75% Analysis Date = 06/17/16 Pct Recovery = 75% Analysis Date = 06/12/16 Pct Recovery = 75% Analysis Date = 06/12/16 Pct Recovery = 75% Analysis Date = 06/08/16 Pct Recovery = 74% Analysis Date = 06/08/16 Pct Recovery = 74% Analysis Date = 06/03/16 Pct Recovery = 74% Analysis Date = 06/03/16 Pct Recovery = 74% Analysis Date = 05/29/16 Pct Recovery = 74% Analysis Date = 05/29/16 Pct Recovery = 74% Analysis Date = 05/24/16 Pct Recovery = 74% Analysis Date = 05/24/16 Pct Recovery = 74% Analysis Date = 05/19/16 Pct Recovery = 73% Analysis Date = 05/19/16 Pct Recovery = 73% Analysis Date = 05/14/16 Pct Recovery = 73% Analysis Date = 05/14/16 Pct Recovery = 73% Analysis Date = 05/09/16 Pct Recovery = 73% Analysis Date = 05/09/16 Pct Recovery = 73% Analysis Date = 05/04/16 Pct Recovery = 73% Analysis Date = 05/04/16 Pct Recovery = 73% Analysis Date = 04/29/16 Pct Recovery = 73% Analysis Date = 04/29/16 Pct Recovery = 73% Analysis Date = 04/25/16 Pct Recovery = 72% Analysis Date = 04/25/16 Pct Recovery = 72% Analysis Date = 04/20/16 Pct Recovery = 72% Analysis Date = 04/20/16 Pct Recovery = 72% Analysis Date = 04/15/16 Pct Recovery = 72% Analysis Date = 04/15/16 Pct Recovery = 72% Analysis Date = 04/10/16 Pct Recovery = 72% Analysis Date = 04/10/16 Pct Recovery = 72% Analysis Date = 04/05/16 Pct Recovery = 71% Analysis Date = 04/05/16 Pct Recovery = 71% Analysis Date = 03/31/16 Pct Recovery = 71% Analysis Date = 03/31/16 Pct Recovery = 71% Analysis Date = 03/26/16 Pct Recovery = 71% Analysis Date = 03/26/16 Pct Recovery = 71% Analysis Date = 03/21/16 Pct Recovery = 71% Analysis Date = 03/21/16 Pct Recovery = 71% Analysis Date = 03/16/16 Pct Recovery = 71% Analysis Date = 03/16/16 Pct Recovery = 71% Analysis Date = 03/12/16 Pct Recovery = 71% Analysis Date = 03/12/16 Pct Recovery = 71% Analysis Date = 03/07/16 Pct Recovery = 71% Analysis Date = 03/07/16 Pct Recovery = 71% Analysis Date = 03/02/16 Pct Recovery = 71% Analysis Date = 03/02/16 Pct Recovery = 71% Analysis Date = 02/26/16 Pct Recovery = 71% Analysis Date = 02/26/16 Pct Recovery = 71% Analysis Date = 02/21/16 Pct Recovery = 71% Analysis Date = 02/21/16 Pct Recovery = 71% Analysis Date = 02/16/16 Pct Recovery = 71% Analysis Date = 02/16/16 Pct Recovery = 71% Analysis Date = 02/11/16 Pct Recovery = 71% Analysis Date = 02/11/16 Pct Recovery = 71% Analysis Date = 02/06/16 Pct Recovery = 71% Analysis Date = 02/06/16 Pct Recovery = 71% Analysis Date = 02/01/16 Pct Recovery = 71% Analysis Date = 02/01/16 Pct Recovery = 71% Analysis Date = 01/28/16 Pct Recovery = 71% Analysis Date = 01/28/16 Pct Recovery = 71% Analysis Date = 01/23/16 Pct Recovery = 71% Analysis Date = 01/23/16 Pct Recovery = 71% Analysis Date = 01/18/16 Pct Recovery = 70% Analysis Date = 01/18/16 Pct Recovery = 70% Analysis Date = 01/13/16 Pct Recovery = 70% Analysis Date = 01/13/16 Pct Recovery = 70% Analysis Date = 01/08/16 Pct Recovery = 70% Analysis Date = 01/08/16 Pct Recovery = 70% Analysis Date = 01/03/16 Pct Recovery = 70% Analysis Date = 01/03/16 Pct Recovery = 70% Analysis Date = 12/29/15 Pct Recovery = 70% Analysis Date = 12/29/15 Pct Recovery = 70% Analysis Date = 12/24/15 Pct Recovery = 70% Analysis Date = 12/24/15 Pct Recovery = 70% Analysis Date = 12/19/15 Pct Recovery = 70% Analysis Date = 12/19/15 Pct Recovery = 70% Analysis Date = 12/15/15 Pct Recovery = 70% Analysis Date = 12/15/15 Pct Recovery = 70% Analysis Date = 12/10/15 Pct Recovery = 70% Analysis Date = 12/10/15 Pct Recovery = 70% Analysis Date = 12/05/15 Pct Recovery = 70% Analysis Date = 12/05/15 Pct Recovery = 70% Analysis Date = 11/30/15 Pct Recovery = 70% Analysis Date = 11/30/15 Pct Recovery = 70% Analysis Date = 11/25/15 Pct Recovery = 70% Analysis Date = 11/25/15 Pct Recovery = 70% Analysis Date = 11/20/15 Pct Recovery = 70% Analysis Date = 11/20/15 Pct Recovery = 70% Analysis Date = 11/15/15 Pct Recovery = 70% Analysis Date = 11/15/15 Pct Recovery = 70% Analysis Date = 11/10/15 Pct Recovery = 70% Analysis Date = 11/10/15 Pct Recovery = 70% Analysis Date = 11/05/15 Pct Recovery = 69% Analysis Date = 11/05/15 Pct Recovery = 69% Analysis Date = 11/01/15 Pct Recovery = 69% Analysis Date = 11/01/15 Pct Recovery = 69% Analysis Date = 10/27/15 Pct Recovery = 69% Analysis Date = 10/27/15 Pct Recovery = 69% Analysis Date = 10/22/15 Pct Recovery = 69% Analysis Date = 10/22/15 Pct Recovery = 69% Analysis Date = 10/17/15 Pct Recovery = 69% Analysis Date = 10/17/15 Pct Recovery = 69% Analysis Date = 10/12/15 Pct Recovery = 69% Analysis Date = 10/12/15 Pct Recovery = 69% Analysis Date = 10/07/15 Pct Recovery = 69% Analysis Date = 10/07/15 Pct Recovery = 69% Analysis Date = 10/02/15 Pct Recovery = 69% Analysis Date = 10/02/15 Pct Recovery = 69% Analysis Date = 09/27/15 Pct Recovery = 69% Analysis Date = 09/27/15 Pct Recovery = 69% Analysis Date = 09/22/15 Pct Recovery = 69% Analysis Date = 09/22/15 Pct Recovery = 69% Analysis Date = 09/17/15 Pct Recovery = 69% Analysis Date = 09/17/15 Pct Recovery = 69% Analysis Date = 09/13/15 Pct Recovery = 70% Analysis Date = 09/13/15 Pct Recovery = 70% Analysis Date = 09/08/15 Pct Recovery = 70% Analysis Date = 09/08/15 Pct Recovery = 70% Analysis Date = 09/03/15 Pct Recovery = 70% Analysis Date = 09/03/15 Pct Recovery = 70% Analysis Date = 08/29/15 Pct Recovery = 70% Analysis Date = 08/29/15 Pct Recovery = 70% Analysis Date = 08/24/15 Pct Recovery = 70% Analysis Date = 08/24/15 Pct Recovery = 70% Analysis Date = 08/19/15 Pct Recovery = 70% Analysis Date = 08/19/15 Pct Recovery = 70% Analysis Date = 08/14/15 Pct Recovery = 71% Analysis Date = 08/14/15 Pct Recovery = 71% Analysis Date = 08/09/15 Pct Recovery = 71% Analysis Date = 08/09/15 Pct Recovery = 71% Analysis Date = 08/04/15 Pct Recovery = 71% Analysis Date = 08/04/15 Pct Recovery = 71% Analysis Date = 07/31/15 Pct Recovery = 71% Analysis Date = 07/31/15 Pct Recovery = 71% Analysis Date = 07/26/15 Pct Recovery = 71% Analysis Date = 07/26/15 Pct Recovery = 71% Analysis Date = 07/21/15 Pct Recovery = 71% Analysis Date = 07/21/15 Pct Recovery = 71% Analysis Date = 07/16/15 Pct Recovery = 71% Analysis Date = 07/16/15 Pct Recovery = 71% Analysis Date = 07/11/15 Pct Recovery = 72% Analysis Date = 07/11/15 Pct Recovery = 72% Analysis Date = 07/06/15 Pct Recovery = 72% Analysis Date = 07/06/15 Pct Recovery = 72% Analysis Date = 07/01/15 Pct Recovery = 72% Analysis Date = 07/01/15 Pct Recovery = 72% Analysis Date = 06/26/15 Pct Recovery = 72% Analysis Date = 06/26/15 Pct Recovery = 72% Analysis Date = 06/21/15 Pct Recovery = 72% Analysis Date = 06/21/15 Pct Recovery = 72% Analysis Date = 06/17/15 Pct Recovery = 72% Analysis Date = 06/17/15 Pct Recovery = 72% Analysis Date = 06/12/15 Pct Recovery = 72% Analysis Date = 06/12/15 Pct Recovery = 72% Analysis Date = 06/07/15 Pct Recovery = 73% Analysis Date = 06/07/15 Pct Recovery = 73% Analysis Date = 06/02/15 Pct Recovery = 73% Analysis Date = 06/02/15 Pct Recovery = 73% Analysis Date = 05/28/15 Pct Recovery = 73% Analysis Date = 05/28/15 Pct Recovery = 73% Analysis Date = 05/23/15 Pct Recovery = 73% Analysis Date = 05/23/15 Pct Recovery = 73% Analysis Date = 05/18/15 Pct Recovery = 73% Analysis Date = 05/18/15 Pct Recovery = 73% Analysis Date = 05/13/15 Pct Recovery = 73% Analysis Date = 05/13/15 Pct Recovery = 73% Analysis Date = 05/08/15 Pct Recovery = 73% Analysis Date = 05/08/15 Pct Recovery = 73% Analysis Date = 05/04/15 Pct Recovery = 74% Analysis Date = 05/04/15 Pct Recovery = 74% Analysis Date = 04/29/15 Pct Recovery = 74% Analysis Date = 04/29/15 Pct Recovery = 74% Analysis Date = 04/24/15 Pct Recovery = 74% Analysis Date = 04/24/15 Pct Recovery = 74% Analysis Date = 04/19/15 Pct Recovery = 74% Analysis Date = 04/19/15 Pct Recovery = 74% Analysis Date = 04/14/15 Pct Recovery = 74% Analysis Date = 04/14/15 Pct Recovery = 74% Analysis Date = 04/09/15 Pct Recovery = 74% Analysis Date = 04/09/15 Pct Recovery = 74% Analysis Date = 04/04/15 Pct Recovery = 74% Analysis Date = 04/04/15 Pct Recovery = 74% Analysis Date = 03/30/15 Pct Recovery = 74% Analysis Date = 03/30/15 Pct Recovery = 74% Analysis Date = 03/25/15 Pct Recovery = 74% Analysis Date = 03/25/15 Pct Recovery = 74% Analysis Date = 03/21/15 Pct Recovery = 74% Analysis Date = 03/21/15 Pct Recovery = 74% Analysis Date = 03/16/15 Pct Recovery = 74% Analysis Date = 03/16/15 Pct Recovery = 74% Analysis Date = 03/11/15 Pct Recovery = 74% Analysis Date = 03/11/15 Pct Recovery = 74% Analysis Date = 03/06/15 Pct Recovery = 74% Analysis Date = 03/06/15 Pct Recovery = 74% Analysis Date = 03/01/15 Pct Recovery = 74% Analysis Date = 03/01/15 Pct Recovery = 74% Analysis Date = 02/24/15 Pct Recovery = 74% Analysis Date = 02/24/15 Pct Recovery = 74% Analysis Date = 02/19/15 Pct Recovery = 74% Analysis Date = 02/19/15 Pct Recovery = 74% Analysis Date = 02/14/15 Pct Recovery = 74% Analysis Date = 02/14/15 Pct Recovery = 74% Analysis Date = 02/09/15 Pct Recovery = 74% Analysis Date = 02/09/15 Pct Recovery = 74% Analysis Date = 02/05/15 Pct Recovery = 74% Analysis Date = 02/05/15 Pct Recovery = 74% Analysis Date = 01/31/15 Pct Recovery = 74% Analysis Date = 01/31/15 Pct Recovery = 74% Analysis Date = 01/26/15 Pct Recovery = 74% Analysis Date = 01/26/15 Pct Recovery = 74% Analysis Date = 01/21/15 Pct Recovery = 73% Analysis Date = 01/21/15 Pct Recovery = 73% Analysis Date = 01/16/15 Pct Recovery = 73% Analysis Date = 01/16/15 Pct Recovery = 73% Analysis Date = 01/11/15 Pct Recovery = 73% Analysis Date = 01/11/15 Pct Recovery = 73% Analysis Date = 01/06/15 Pct Recovery = 73% Analysis Date = 01/06/15 Pct Recovery = 73% Analysis Date = 01/01/15 Pct Recovery = 73% Analysis Date = 01/01/15 Pct Recovery = 73% Analysis Date = 12/27/14 Pct Recovery = 73% Analysis Date = 12/27/14 Pct Recovery = 73% Analysis Date = 12/23/14 Pct Recovery = 73% Analysis Date = 12/23/14 Pct Recovery = 73% Analysis Date = 12/18/14 Pct Recovery = 73% Analysis Date = 12/18/14 Pct Recovery = 73% Analysis Date = 12/13/14 Pct Recovery = 73% Analysis Date = 12/13/14 Pct Recovery = 73% Analysis Date = 12/08/14 Pct Recovery = 72% Analysis Date = 12/08/14 Pct Recovery = 72% Analysis Date = 12/03/14 Pct Recovery = 72% Analysis Date = 12/03/14 Pct Recovery = 72% Analysis Date = 11/28/14 Pct Recovery = 72% Analysis Date = 11/28/14 Pct Recovery = 72% Analysis Date = 11/23/14 Pct Recovery = 72% Analysis Date = 11/23/14 Pct Recovery = 72% Analysis Date = 11/18/14 Pct Recovery = 72% Analysis Date = 11/18/14 Pct Recovery = 72% Analysis Date = 11/13/14 Pct Recovery = 72% Analysis Date = 11/13/14 Pct Recovery = 72% Analysis Date = 11/09/14 Pct Recovery = 72% Analysis Date = 11/09/14 Pct Recovery = 72% Analysis Date = 11/04/14 Pct Recovery = 72% Analysis Date = 11/04/14 Pct Recovery = 72% Analysis Date = 10/30/14 Pct Recovery = 71% Analysis Date = 10/30/14 Pct Recovery = 71% Analysis Date = 10/25/14 Pct Recovery = 71% Analysis Date = 10/25/14 Pct Recovery = 71% Analysis Date = 10/20/14 Pct Recovery = 71% Analysis Date = 10/20/14 Pct Recovery = 71% Analysis Date = 10/15/14 Pct Recovery = 71% Analysis Date = 10/15/14 Pct Recovery = 71% Analysis Date = 10/10/14 Pct Recovery = 71% Analysis Date = 10/10/14 Pct Recovery = 71% Analysis Date = 10/05/14 Pct Recovery = 71% Analysis Date = 10/05/14 Pct Recovery = 71% Analysis Date = 09/30/14 Pct Recovery = 70% Analysis Date = 09/30/14 Pct Recovery = 70% Analysis Date = 09/26/14 Pct Recovery = 70% Analysis Date = 09/26/14 Pct Recovery = 70% Analysis Date = 09/21/14 Pct Recovery = 70% Analysis Date = 09/21/14 Pct Recovery = 70% Analysis Date = 09/16/14 Pct Recovery = 70% Analysis Date = 09/16/14 Pct Recovery = 70% Analysis Date = 09/11/14 Pct Recovery = 70% Analysis Date = 09/11/14 Pct Recovery = 70% Analysis Date = 09/06/14 Pct Recovery = 69% Analysis Date = 09/06/14 Pct Recovery = 69% Analysis Date = 09/01/14 Pct Recovery = 69% Analysis Date = 09/01/14 Pct Recovery = 69% Analysis Date = 08/27/14 Pct Recovery = 69% Analysis Date = 08/27/14 Pct Recovery = 69% Analysis Date = 08/22/14 Pct Recovery = 69% Analysis Date = 08/22/14 Pct Recovery = 69% Analysis Date = 08/17/14 Pct Recovery = 69% Analysis Date = 08/17/14 Pct Recovery = 69% Analysis Date = 08/13/14 Pct Recovery = 68% Analysis Date = 08/13/14 Pct Recovery = 68% Analysis Date = 08/08/14 Pct Recovery = 68% Analysis Date = 08/08/14 Pct Recovery = 68% Analysis Date = 08/03/14 Pct Recovery = 68% Analysis Date = 08/03/14 Pct Recovery = 68% Analysis Date = 07/29/14 Pct Recovery = 68% Analysis Date = 07/29/14 Pct Recovery = 68% Analysis Date = 07/24/14 Pct Recovery = 68% Analysis Date = 07/24/14 Pct Recovery = 68% Analysis Date = 07/19/14 Pct Recovery = 67% Analysis Date = 07/19/14 Pct Recovery = 67% Analysis Date = 07/14/14 Pct Recovery = 67% Analysis Date = 07/14/14 Pct Recovery = 67% Analysis Date = 07/09/14 Pct Recovery = 67% Analysis Date = 07/09/14 Pct Recovery = 67% Analysis Date = 07/04/14 Pct Recovery = 67% Analysis Date = 07/04/14 Pct Recovery = 67% Analysis Date = 06/30/14 Pct Recovery = 66% Analysis Date = 06/30/14 Pct Recovery = 66% Analysis Date = 06/25/14 Pct Recovery = 66% Analysis Date = 06/25/14 Pct Recovery = 66% Analysis Date = 06/20/14 Pct Recovery = 66% Analysis Date = 06/20/14 Pct Recovery = 66% Analysis Date = 06/15/14 Pct Recovery = 66% Analysis Date = 06/15/14 Pct Recovery = 66% Analysis Date = 06/10/14 Pct Recovery = 65% Analysis Date = 06/10/14 Pct Recovery = 65% Analysis Date = 06/05/14 Pct Recovery = 65% Analysis Date = 06/05/14 Pct Recovery = 65% Analysis Date = 05/31/14 Pct Recovery = 65% Analysis Date = 05/31/14 Pct Recovery = 65% Analysis Date = 05/26/14 Pct Recovery = 64% Analysis Date = 05/26/14 Pct Recovery = 64% Analysis Date = 05/21/14 Pct Recovery = 64% Analysis Date = 05/21/14 Pct Recovery = 64% Analysis Date = 05/17/14 Pct Recovery = 64% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
SITAGLIPTIN

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 2 104% 34% 104% 36%
>= Reporting Level 61 74% 20% 74% 15%
Total 63 75% 21% 74% 16%

Sample Statistics
SITAGLIPTIN

Characteristic N % % Basis
Plotted 63 100% Spiked
Estimated Values 21 33% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 63 .  
False Negatives 0 0% 0 out of 63
Not Spiked 52 .  
False Positives 0 0% 0 out of 52

BQS OBSP Determination:
SULFADIMETHOXINE
METHOD: 2440 , TESTIDCODE: 67503LCM56
Open Data Set

Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 92% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 91% Analysis Date = 01/17/16 SpikeMix = ERA 0406-15-09: 80 µl & ERA 0406-15-07A: 80 µl Pct Recovery = 81% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 80 µl & Abs 051315: 80 µl Pct Recovery = 81% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 80 µl & ERA 0406-15-08: 80 µl Pct Recovery = 87% Analysis Date = 11/04/15 SpikeMix = Abs 052215: 80 µl & Abs 050115: 80 µl Pct Recovery = 85% Analysis Date = 09/24/16 SpikeMix = Crescent EN160610015: 80 µl & Abs 061416: 80 µl Pct Recovery = 97% Analysis Date = 09/24/16 SpikeMix = Abs 061416: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 94% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 110% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 107% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 107% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 105% Analysis Date = 11/18/16 SpikeMix = ERA 04281604: 80 µl & ERA 04281603: 80 µl Pct Recovery = 86% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & ERA 04281604: 80 µl Pct Recovery = 90% Analysis Date = 05/07/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 94% Analysis Date = 03/11/15 SpikeMix = ERA 0318-14-02: 15 µl & Abs 041714: 15 µl Pct Recovery = 82% Analysis Date = 01/16/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 82% Analysis Date = 12/06/14 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 69% Analysis Date = 08/21/14 SpikeMix = ERA 0318-14-02: 60 µl & Abs 041714: 60 µl Pct Recovery = 61% Analysis Date = 07/12/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 65% Analysis Date = 06/11/14 SpikeMix = Abs 041614: 60 µl & Abs 041714: 60 µl Pct Recovery = 76% Analysis Date = 05/21/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 79% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-04: 15 µl & Abs 041814: 15 µl Pct Recovery = 83% Analysis Date = 12/06/14 SpikeMix = ERA 0318-14-02: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 79% Analysis Date = 10/25/14 SpikeMix = Abs 041614: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 80% Analysis Date = 10/11/14 SpikeMix = ERA 0318-14-02: 60 µl & ERA 0319-14-04: 60 µl Pct Recovery = 72% Analysis Date = 08/28/14 SpikeMix = ERA 0319-14-04: 60 µl & ERA 0319-14-05: 60 µl Pct Recovery = 77% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-07A: 40 µl & Abs 051315: 40 µl Pct Recovery = 82% Analysis Date = 11/04/15 SpikeMix = ERA 0406-15-07A: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 79% Analysis Date = 09/10/15 SpikeMix = Abs 052215: 40 µl & ERA 0406-15-07A: 40 µl Pct Recovery = 106% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 85% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 70% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 80% Analysis Date = 02/23/16 SpikeMix = Abs 052215: 40 µl & Abs 050115: 40 µl Pct Recovery = 86% Analysis Date = 07/31/15 SpikeMix = ERA 0406-15-09: 40 µl & Abs 050115: 40 µl Pct Recovery = 96% Analysis Date = 07/30/15 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 86% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 82% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 83% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 79% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 79% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 77% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 83% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 84% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 82% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 113% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 120% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 103% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 96% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 84% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 87% Analysis Date = 11/04/14 SpikeMix = Abs 041714: 8 µl & ERA 0319-14-05: 8 µl Pct Recovery = 69% Analysis Date = 04/30/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 112% Analysis Date = 04/10/15 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 80% Analysis Date = 02/10/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 95% Analysis Date = 12/07/14 SpikeMix = ERA 0318-14-02: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 76% Analysis Date = 10/11/14 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 70% Analysis Date = 10/10/14 SpikeMix = Abs 041714: 30 µl & Abs 041814: 30 µl Pct Recovery = 64% Analysis Date = 07/20/14 SpikeMix = ERA 0318-14-02: 30 µl & Abs 041714: 30 µl Pct Recovery = 63% Analysis Date = 06/28/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 64% Analysis Date = 05/17/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 66% Analysis Date = 09/12/14 SpikeMix = Abs 041614: 30 µl & ERA 0319-14-04: 30 µl Pct Recovery = 65% Analysis Date = 08/16/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 68% Analysis Date = 07/13/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 75% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 57% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 63% Analysis Date = 04/27/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 110% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 67% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 63% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 64% Analysis Date = 11/24/15 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 89% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-09: 20 µl Pct Recovery = 19% Analysis Date = 09/15/15 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 80% Analysis Date = 11/25/15 SpikeMix = Abs 050115: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 94% Analysis Date = 11/24/15 SpikeMix = ERA 0406-15-09: 20 µl & Abs 050115: 20 µl Pct Recovery = 87% Analysis Date = 08/27/15 SpikeMix = Abs 052215: 20 µl & Abs 050115: 20 µl Pct Recovery = 83% Analysis Date = 08/11/15 SpikeMix = Abs 050115: 20 µl & Abs 051315: 20 µl Pct Recovery = 63% Analysis Date = 07/09/15 SpikeMix = Abs 050115: 20 µl & Abs 052215: 20 µl Pct Recovery = 86% Analysis Date = 06/09/15 SpikeMix = Abs 051315: 20 µl & Abs 050115: 20 µl Pct Recovery = 83% Analysis Date = 01/04/17 Pct Recovery = 98% Analysis Date = 12/31/16 Pct Recovery = 98% Analysis Date = 12/31/16 Pct Recovery = 98% Analysis Date = 12/26/16 Pct Recovery = 97% Analysis Date = 12/26/16 Pct Recovery = 97% Analysis Date = 12/21/16 Pct Recovery = 97% Analysis Date = 12/21/16 Pct Recovery = 97% Analysis Date = 12/16/16 Pct Recovery = 97% Analysis Date = 12/16/16 Pct Recovery = 97% Analysis Date = 12/11/16 Pct Recovery = 96% Analysis Date = 12/11/16 Pct Recovery = 96% Analysis Date = 12/07/16 Pct Recovery = 96% Analysis Date = 12/07/16 Pct Recovery = 96% Analysis Date = 12/02/16 Pct Recovery = 96% Analysis Date = 12/02/16 Pct Recovery = 96% Analysis Date = 11/27/16 Pct Recovery = 95% Analysis Date = 11/27/16 Pct Recovery = 95% Analysis Date = 11/22/16 Pct Recovery = 95% Analysis Date = 11/22/16 Pct Recovery = 95% Analysis Date = 11/17/16 Pct Recovery = 95% Analysis Date = 11/17/16 Pct Recovery = 95% Analysis Date = 11/12/16 Pct Recovery = 94% Analysis Date = 11/12/16 Pct Recovery = 94% Analysis Date = 11/08/16 Pct Recovery = 94% Analysis Date = 11/08/16 Pct Recovery = 94% Analysis Date = 11/03/16 Pct Recovery = 94% Analysis Date = 11/03/16 Pct Recovery = 94% Analysis Date = 10/29/16 Pct Recovery = 93% Analysis Date = 10/29/16 Pct Recovery = 93% Analysis Date = 10/24/16 Pct Recovery = 93% Analysis Date = 10/24/16 Pct Recovery = 93% Analysis Date = 10/19/16 Pct Recovery = 93% Analysis Date = 10/19/16 Pct Recovery = 93% Analysis Date = 10/15/16 Pct Recovery = 92% Analysis Date = 10/15/16 Pct Recovery = 92% Analysis Date = 10/10/16 Pct Recovery = 92% Analysis Date = 10/10/16 Pct Recovery = 92% Analysis Date = 10/05/16 Pct Recovery = 92% Analysis Date = 10/05/16 Pct Recovery = 92% Analysis Date = 09/30/16 Pct Recovery = 91% Analysis Date = 09/30/16 Pct Recovery = 91% Analysis Date = 09/25/16 Pct Recovery = 91% Analysis Date = 09/25/16 Pct Recovery = 91% Analysis Date = 09/20/16 Pct Recovery = 91% Analysis Date = 09/20/16 Pct Recovery = 91% Analysis Date = 09/16/16 Pct Recovery = 91% Analysis Date = 09/16/16 Pct Recovery = 91% Analysis Date = 09/11/16 Pct Recovery = 90% Analysis Date = 09/11/16 Pct Recovery = 90% Analysis Date = 09/06/16 Pct Recovery = 90% Analysis Date = 09/06/16 Pct Recovery = 90% Analysis Date = 09/01/16 Pct Recovery = 90% Analysis Date = 09/01/16 Pct Recovery = 90% Analysis Date = 08/27/16 Pct Recovery = 89% Analysis Date = 08/27/16 Pct Recovery = 89% Analysis Date = 08/23/16 Pct Recovery = 89% Analysis Date = 08/23/16 Pct Recovery = 89% Analysis Date = 08/18/16 Pct Recovery = 89% Analysis Date = 08/18/16 Pct Recovery = 89% Analysis Date = 08/13/16 Pct Recovery = 88% Analysis Date = 08/13/16 Pct Recovery = 88% Analysis Date = 08/08/16 Pct Recovery = 88% Analysis Date = 08/08/16 Pct Recovery = 88% Analysis Date = 08/03/16 Pct Recovery = 88% Analysis Date = 08/03/16 Pct Recovery = 88% Analysis Date = 07/29/16 Pct Recovery = 88% Analysis Date = 07/29/16 Pct Recovery = 88% Analysis Date = 07/25/16 Pct Recovery = 87% Analysis Date = 07/25/16 Pct Recovery = 87% Analysis Date = 07/20/16 Pct Recovery = 87% Analysis Date = 07/20/16 Pct Recovery = 87% Analysis Date = 07/15/16 Pct Recovery = 87% Analysis Date = 07/15/16 Pct Recovery = 87% Analysis Date = 07/10/16 Pct Recovery = 87% Analysis Date = 07/10/16 Pct Recovery = 87% Analysis Date = 07/05/16 Pct Recovery = 86% Analysis Date = 07/05/16 Pct Recovery = 86% Analysis Date = 07/01/16 Pct Recovery = 86% Analysis Date = 07/01/16 Pct Recovery = 86% Analysis Date = 06/26/16 Pct Recovery = 86% Analysis Date = 06/26/16 Pct Recovery = 86% Analysis Date = 06/21/16 Pct Recovery = 85% Analysis Date = 06/21/16 Pct Recovery = 85% Analysis Date = 06/16/16 Pct Recovery = 85% Analysis Date = 06/16/16 Pct Recovery = 85% Analysis Date = 06/11/16 Pct Recovery = 85% Analysis Date = 06/11/16 Pct Recovery = 85% Analysis Date = 06/06/16 Pct Recovery = 85% Analysis Date = 06/06/16 Pct Recovery = 85% Analysis Date = 06/02/16 Pct Recovery = 84% Analysis Date = 06/02/16 Pct Recovery = 84% Analysis Date = 05/28/16 Pct Recovery = 84% Analysis Date = 05/28/16 Pct Recovery = 84% Analysis Date = 05/23/16 Pct Recovery = 84% Analysis Date = 05/23/16 Pct Recovery = 84% Analysis Date = 05/18/16 Pct Recovery = 84% Analysis Date = 05/18/16 Pct Recovery = 84% Analysis Date = 05/13/16 Pct Recovery = 83% Analysis Date = 05/13/16 Pct Recovery = 83% Analysis Date = 05/08/16 Pct Recovery = 83% Analysis Date = 05/08/16 Pct Recovery = 83% Analysis Date = 05/04/16 Pct Recovery = 83% Analysis Date = 05/04/16 Pct Recovery = 83% Analysis Date = 04/29/16 Pct Recovery = 83% Analysis Date = 04/29/16 Pct Recovery = 83% Analysis Date = 04/24/16 Pct Recovery = 83% Analysis Date = 04/24/16 Pct Recovery = 83% Analysis Date = 04/19/16 Pct Recovery = 83% Analysis Date = 04/19/16 Pct Recovery = 83% Analysis Date = 04/14/16 Pct Recovery = 83% Analysis Date = 04/14/16 Pct Recovery = 83% Analysis Date = 04/10/16 Pct Recovery = 82% Analysis Date = 04/10/16 Pct Recovery = 82% Analysis Date = 04/05/16 Pct Recovery = 82% Analysis Date = 04/05/16 Pct Recovery = 82% Analysis Date = 03/31/16 Pct Recovery = 82% Analysis Date = 03/31/16 Pct Recovery = 82% Analysis Date = 03/26/16 Pct Recovery = 82% Analysis Date = 03/26/16 Pct Recovery = 82% Analysis Date = 03/21/16 Pct Recovery = 82% Analysis Date = 03/21/16 Pct Recovery = 82% Analysis Date = 03/16/16 Pct Recovery = 82% Analysis Date = 03/16/16 Pct Recovery = 82% Analysis Date = 03/12/16 Pct Recovery = 82% Analysis Date = 03/12/16 Pct Recovery = 82% Analysis Date = 03/07/16 Pct Recovery = 81% Analysis Date = 03/07/16 Pct Recovery = 81% Analysis Date = 03/02/16 Pct Recovery = 81% Analysis Date = 03/02/16 Pct Recovery = 81% Analysis Date = 02/26/16 Pct Recovery = 81% Analysis Date = 02/26/16 Pct Recovery = 81% Analysis Date = 02/21/16 Pct Recovery = 81% Analysis Date = 02/21/16 Pct Recovery = 81% Analysis Date = 02/17/16 Pct Recovery = 81% Analysis Date = 02/17/16 Pct Recovery = 81% Analysis Date = 02/12/16 Pct Recovery = 81% Analysis Date = 02/12/16 Pct Recovery = 81% Analysis Date = 02/07/16 Pct Recovery = 81% Analysis Date = 02/07/16 Pct Recovery = 81% Analysis Date = 02/02/16 Pct Recovery = 81% Analysis Date = 02/02/16 Pct Recovery = 81% Analysis Date = 01/28/16 Pct Recovery = 81% Analysis Date = 01/28/16 Pct Recovery = 81% Analysis Date = 01/23/16 Pct Recovery = 81% Analysis Date = 01/23/16 Pct Recovery = 81% Analysis Date = 01/19/16 Pct Recovery = 81% Analysis Date = 01/19/16 Pct Recovery = 81% Analysis Date = 01/14/16 Pct Recovery = 81% Analysis Date = 01/14/16 Pct Recovery = 81% Analysis Date = 01/09/16 Pct Recovery = 81% Analysis Date = 01/09/16 Pct Recovery = 81% Analysis Date = 01/04/16 Pct Recovery = 81% Analysis Date = 01/04/16 Pct Recovery = 81% Analysis Date = 12/30/15 Pct Recovery = 81% Analysis Date = 12/30/15 Pct Recovery = 81% Analysis Date = 12/26/15 Pct Recovery = 81% Analysis Date = 12/26/15 Pct Recovery = 81% Analysis Date = 12/21/15 Pct Recovery = 81% Analysis Date = 12/21/15 Pct Recovery = 81% Analysis Date = 12/16/15 Pct Recovery = 81% Analysis Date = 12/16/15 Pct Recovery = 81% Analysis Date = 12/11/15 Pct Recovery = 81% Analysis Date = 12/11/15 Pct Recovery = 81% Analysis Date = 12/06/15 Pct Recovery = 81% Analysis Date = 12/06/15 Pct Recovery = 81% Analysis Date = 12/01/15 Pct Recovery = 81% Analysis Date = 12/01/15 Pct Recovery = 81% Analysis Date = 11/27/15 Pct Recovery = 81% Analysis Date = 11/27/15 Pct Recovery = 81% Analysis Date = 11/22/15 Pct Recovery = 81% Analysis Date = 11/22/15 Pct Recovery = 81% Analysis Date = 11/17/15 Pct Recovery = 81% Analysis Date = 11/17/15 Pct Recovery = 81% Analysis Date = 11/12/15 Pct Recovery = 81% Analysis Date = 11/12/15 Pct Recovery = 81% Analysis Date = 11/07/15 Pct Recovery = 81% Analysis Date = 11/07/15 Pct Recovery = 81% Analysis Date = 11/03/15 Pct Recovery = 81% Analysis Date = 11/03/15 Pct Recovery = 81% Analysis Date = 10/29/15 Pct Recovery = 81% Analysis Date = 10/29/15 Pct Recovery = 81% Analysis Date = 10/24/15 Pct Recovery = 81% Analysis Date = 10/24/15 Pct Recovery = 81% Analysis Date = 10/19/15 Pct Recovery = 81% Analysis Date = 10/19/15 Pct Recovery = 81% Analysis Date = 10/14/15 Pct Recovery = 81% Analysis Date = 10/14/15 Pct Recovery = 81% Analysis Date = 10/09/15 Pct Recovery = 81% Analysis Date = 10/09/15 Pct Recovery = 81% Analysis Date = 10/05/15 Pct Recovery = 81% Analysis Date = 10/05/15 Pct Recovery = 81% Analysis Date = 09/30/15 Pct Recovery = 82% Analysis Date = 09/30/15 Pct Recovery = 82% Analysis Date = 09/25/15 Pct Recovery = 82% Analysis Date = 09/25/15 Pct Recovery = 82% Analysis Date = 09/20/15 Pct Recovery = 82% Analysis Date = 09/20/15 Pct Recovery = 82% Analysis Date = 09/15/15 Pct Recovery = 82% Analysis Date = 09/15/15 Pct Recovery = 82% Analysis Date = 09/10/15 Pct Recovery = 82% Analysis Date = 09/10/15 Pct Recovery = 82% Analysis Date = 09/06/15 Pct Recovery = 82% Analysis Date = 09/06/15 Pct Recovery = 82% Analysis Date = 09/01/15 Pct Recovery = 82% Analysis Date = 09/01/15 Pct Recovery = 82% Analysis Date = 08/27/15 Pct Recovery = 82% Analysis Date = 08/27/15 Pct Recovery = 82% Analysis Date = 08/22/15 Pct Recovery = 82% Analysis Date = 08/22/15 Pct Recovery = 82% Analysis Date = 08/17/15 Pct Recovery = 82% Analysis Date = 08/17/15 Pct Recovery = 82% Analysis Date = 08/13/15 Pct Recovery = 82% Analysis Date = 08/13/15 Pct Recovery = 82% Analysis Date = 08/08/15 Pct Recovery = 83% Analysis Date = 08/08/15 Pct Recovery = 83% Analysis Date = 08/03/15 Pct Recovery = 83% Analysis Date = 08/03/15 Pct Recovery = 83% Analysis Date = 07/29/15 Pct Recovery = 83% Analysis Date = 07/29/15 Pct Recovery = 83% Analysis Date = 07/24/15 Pct Recovery = 83% Analysis Date = 07/24/15 Pct Recovery = 83% Analysis Date = 07/19/15 Pct Recovery = 82% Analysis Date = 07/19/15 Pct Recovery = 82% Analysis Date = 07/15/15 Pct Recovery = 82% Analysis Date = 07/15/15 Pct Recovery = 82% Analysis Date = 07/10/15 Pct Recovery = 82% Analysis Date = 07/10/15 Pct Recovery = 82% Analysis Date = 07/05/15 Pct Recovery = 82% Analysis Date = 07/05/15 Pct Recovery = 82% Analysis Date = 06/30/15 Pct Recovery = 82% Analysis Date = 06/30/15 Pct Recovery = 82% Analysis Date = 06/25/15 Pct Recovery = 82% Analysis Date = 06/25/15 Pct Recovery = 82% Analysis Date = 06/21/15 Pct Recovery = 82% Analysis Date = 06/21/15 Pct Recovery = 82% Analysis Date = 06/16/15 Pct Recovery = 82% Analysis Date = 06/16/15 Pct Recovery = 82% Analysis Date = 06/11/15 Pct Recovery = 82% Analysis Date = 06/11/15 Pct Recovery = 82% Analysis Date = 06/06/15 Pct Recovery = 82% Analysis Date = 06/06/15 Pct Recovery = 82% Analysis Date = 06/01/15 Pct Recovery = 82% Analysis Date = 06/01/15 Pct Recovery = 82% Analysis Date = 05/27/15 Pct Recovery = 81% Analysis Date = 05/27/15 Pct Recovery = 81% Analysis Date = 05/23/15 Pct Recovery = 81% Analysis Date = 05/23/15 Pct Recovery = 81% Analysis Date = 05/18/15 Pct Recovery = 81% Analysis Date = 05/18/15 Pct Recovery = 81% Analysis Date = 05/13/15 Pct Recovery = 81% Analysis Date = 05/13/15 Pct Recovery = 81% Analysis Date = 05/08/15 Pct Recovery = 81% Analysis Date = 05/08/15 Pct Recovery = 81% Analysis Date = 05/03/15 Pct Recovery = 81% Analysis Date = 05/03/15 Pct Recovery = 81% Analysis Date = 04/29/15 Pct Recovery = 81% Analysis Date = 04/29/15 Pct Recovery = 81% Analysis Date = 04/24/15 Pct Recovery = 81% Analysis Date = 04/24/15 Pct Recovery = 81% Analysis Date = 04/19/15 Pct Recovery = 81% Analysis Date = 04/19/15 Pct Recovery = 81% Analysis Date = 04/14/15 Pct Recovery = 80% Analysis Date = 04/14/15 Pct Recovery = 80% Analysis Date = 04/09/15 Pct Recovery = 80% Analysis Date = 04/09/15 Pct Recovery = 80% Analysis Date = 04/04/15 Pct Recovery = 80% Analysis Date = 04/04/15 Pct Recovery = 80% Analysis Date = 03/31/15 Pct Recovery = 80% Analysis Date = 03/31/15 Pct Recovery = 80% Analysis Date = 03/26/15 Pct Recovery = 80% Analysis Date = 03/26/15 Pct Recovery = 80% Analysis Date = 03/21/15 Pct Recovery = 80% Analysis Date = 03/21/15 Pct Recovery = 80% Analysis Date = 03/16/15 Pct Recovery = 79% Analysis Date = 03/16/15 Pct Recovery = 79% Analysis Date = 03/11/15 Pct Recovery = 79% Analysis Date = 03/11/15 Pct Recovery = 79% Analysis Date = 03/07/15 Pct Recovery = 79% Analysis Date = 03/07/15 Pct Recovery = 79% Analysis Date = 03/02/15 Pct Recovery = 79% Analysis Date = 03/02/15 Pct Recovery = 79% Analysis Date = 02/25/15 Pct Recovery = 79% Analysis Date = 02/25/15 Pct Recovery = 79% Analysis Date = 02/20/15 Pct Recovery = 79% Analysis Date = 02/20/15 Pct Recovery = 79% Analysis Date = 02/15/15 Pct Recovery = 79% Analysis Date = 02/15/15 Pct Recovery = 79% Analysis Date = 02/10/15 Pct Recovery = 78% Analysis Date = 02/10/15 Pct Recovery = 78% Analysis Date = 02/06/15 Pct Recovery = 78% Analysis Date = 02/06/15 Pct Recovery = 78% Analysis Date = 02/01/15 Pct Recovery = 78% Analysis Date = 02/01/15 Pct Recovery = 78% Analysis Date = 01/27/15 Pct Recovery = 78% Analysis Date = 01/27/15 Pct Recovery = 78% Analysis Date = 01/22/15 Pct Recovery = 78% Analysis Date = 01/22/15 Pct Recovery = 78% Analysis Date = 01/17/15 Pct Recovery = 78% Analysis Date = 01/17/15 Pct Recovery = 78% Analysis Date = 01/12/15 Pct Recovery = 77% Analysis Date = 01/12/15 Pct Recovery = 77% Analysis Date = 01/08/15 Pct Recovery = 77% Analysis Date = 01/08/15 Pct Recovery = 77% Analysis Date = 01/03/15 Pct Recovery = 77% Analysis Date = 01/03/15 Pct Recovery = 77% Analysis Date = 12/29/14 Pct Recovery = 77% Analysis Date = 12/29/14 Pct Recovery = 77% Analysis Date = 12/24/14 Pct Recovery = 77% Analysis Date = 12/24/14 Pct Recovery = 77% Analysis Date = 12/19/14 Pct Recovery = 76% Analysis Date = 12/19/14 Pct Recovery = 76% Analysis Date = 12/15/14 Pct Recovery = 76% Analysis Date = 12/15/14 Pct Recovery = 76% Analysis Date = 12/10/14 Pct Recovery = 76% Analysis Date = 12/10/14 Pct Recovery = 76% Analysis Date = 12/05/14 Pct Recovery = 76% Analysis Date = 12/05/14 Pct Recovery = 76% Analysis Date = 11/30/14 Pct Recovery = 76% Analysis Date = 11/30/14 Pct Recovery = 76% Analysis Date = 11/25/14 Pct Recovery = 76% Analysis Date = 11/25/14 Pct Recovery = 76% Analysis Date = 11/20/14 Pct Recovery = 75% Analysis Date = 11/20/14 Pct Recovery = 75% Analysis Date = 11/16/14 Pct Recovery = 75% Analysis Date = 11/16/14 Pct Recovery = 75% Analysis Date = 11/11/14 Pct Recovery = 75% Analysis Date = 11/11/14 Pct Recovery = 75% Analysis Date = 11/06/14 Pct Recovery = 75% Analysis Date = 11/06/14 Pct Recovery = 75% Analysis Date = 11/01/14 Pct Recovery = 75% Analysis Date = 11/01/14 Pct Recovery = 75% Analysis Date = 10/27/14 Pct Recovery = 74% Analysis Date = 10/27/14 Pct Recovery = 74% Analysis Date = 10/23/14 Pct Recovery = 74% Analysis Date = 10/23/14 Pct Recovery = 74% Analysis Date = 10/18/14 Pct Recovery = 74% Analysis Date = 10/18/14 Pct Recovery = 74% Analysis Date = 10/13/14 Pct Recovery = 74% Analysis Date = 10/13/14 Pct Recovery = 74% Analysis Date = 10/08/14 Pct Recovery = 74% Analysis Date = 10/08/14 Pct Recovery = 74% Analysis Date = 10/03/14 Pct Recovery = 73% Analysis Date = 10/03/14 Pct Recovery = 73% Analysis Date = 09/28/14 Pct Recovery = 73% Analysis Date = 09/28/14 Pct Recovery = 73% Analysis Date = 09/24/14 Pct Recovery = 73% Analysis Date = 09/24/14 Pct Recovery = 73% Analysis Date = 09/19/14 Pct Recovery = 73% Analysis Date = 09/19/14 Pct Recovery = 73% Analysis Date = 09/14/14 Pct Recovery = 73% Analysis Date = 09/14/14 Pct Recovery = 73% Analysis Date = 09/09/14 Pct Recovery = 72% Analysis Date = 09/09/14 Pct Recovery = 72% Analysis Date = 09/04/14 Pct Recovery = 72% Analysis Date = 09/04/14 Pct Recovery = 72% Analysis Date = 08/31/14 Pct Recovery = 72% Analysis Date = 08/31/14 Pct Recovery = 72% Analysis Date = 08/26/14 Pct Recovery = 72% Analysis Date = 08/26/14 Pct Recovery = 72% Analysis Date = 08/21/14 Pct Recovery = 72% Analysis Date = 08/21/14 Pct Recovery = 72% Analysis Date = 08/16/14 Pct Recovery = 71% Analysis Date = 08/16/14 Pct Recovery = 71% Analysis Date = 08/11/14 Pct Recovery = 71% Analysis Date = 08/11/14 Pct Recovery = 71% Analysis Date = 08/06/14 Pct Recovery = 71% Analysis Date = 08/06/14 Pct Recovery = 71% Analysis Date = 08/02/14 Pct Recovery = 71% Analysis Date = 08/02/14 Pct Recovery = 71% Analysis Date = 07/28/14 Pct Recovery = 71% Analysis Date = 07/28/14 Pct Recovery = 71% Analysis Date = 07/23/14 Pct Recovery = 70% Analysis Date = 07/23/14 Pct Recovery = 70% Analysis Date = 07/18/14 Pct Recovery = 70% Analysis Date = 07/18/14 Pct Recovery = 70% Analysis Date = 07/13/14 Pct Recovery = 70% Analysis Date = 07/13/14 Pct Recovery = 70% Analysis Date = 07/09/14 Pct Recovery = 70% Analysis Date = 07/09/14 Pct Recovery = 70% Analysis Date = 07/04/14 Pct Recovery = 69% Analysis Date = 07/04/14 Pct Recovery = 69% Analysis Date = 06/29/14 Pct Recovery = 69% Analysis Date = 06/29/14 Pct Recovery = 69% Analysis Date = 06/24/14 Pct Recovery = 69% Analysis Date = 06/24/14 Pct Recovery = 69% Analysis Date = 06/19/14 Pct Recovery = 69% Analysis Date = 06/19/14 Pct Recovery = 69% Analysis Date = 06/14/14 Pct Recovery = 69% Analysis Date = 06/14/14 Pct Recovery = 69% Analysis Date = 06/10/14 Pct Recovery = 68% Analysis Date = 06/10/14 Pct Recovery = 68% Analysis Date = 06/05/14 Pct Recovery = 68% Analysis Date = 06/05/14 Pct Recovery = 68% Analysis Date = 05/31/14 Pct Recovery = 68% Analysis Date = 05/31/14 Pct Recovery = 68% Analysis Date = 05/26/14 Pct Recovery = 68% Analysis Date = 05/26/14 Pct Recovery = 68% Analysis Date = 05/21/14 Pct Recovery = 67% Analysis Date = 05/21/14 Pct Recovery = 67% Analysis Date = 05/17/14 Pct Recovery = 67% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
SULFADIMETHOXINE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 78 82% 16% 82% 13%
Total 78 82% 16% 82% 13%

Sample Statistics
SULFADIMETHOXINE

Characteristic N % % Basis
Plotted 78 100% Spiked
Estimated Values 11 14% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 78 .  
False Negatives 0 0% 0 out of 78
Not Spiked 37 .  
False Positives 0 0% 0 out of 37

BQS OBSP Determination:
SULFAMETHIZOLE
METHOD: 2440 , TESTIDCODE: 67476LCM56
Open Data Set

Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 88% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 85% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 80% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 74% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 80 µl & ERA 0406-15-08: 80 µl Pct Recovery = 82% Analysis Date = 11/04/15 SpikeMix = Abs 052215: 80 µl & Abs 050115: 80 µl Pct Recovery = 91% Analysis Date = 01/17/16 SpikeMix = ERA 0406-15-09: 80 µl & ERA 0406-15-07A: 80 µl Pct Recovery = 69% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 80 µl & Abs 051315: 80 µl Pct Recovery = 79% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 75% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 74% Analysis Date = 09/24/16 SpikeMix = Crescent EN160610015: 80 µl & Abs 061416: 80 µl Pct Recovery = 75% Analysis Date = 09/24/16 SpikeMix = Abs 061416: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 71% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 78% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 78% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 87% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 80% Analysis Date = 05/07/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 117% Analysis Date = 03/11/15 SpikeMix = ERA 0318-14-02: 15 µl & Abs 041714: 15 µl Pct Recovery = 82% Analysis Date = 01/16/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 82% Analysis Date = 12/06/14 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 77% Analysis Date = 08/21/14 SpikeMix = ERA 0318-14-02: 60 µl & Abs 041714: 60 µl Pct Recovery = 82% Analysis Date = 07/12/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 65% Analysis Date = 06/11/14 SpikeMix = Abs 041614: 60 µl & Abs 041714: 60 µl Pct Recovery = 100% Analysis Date = 05/21/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 87% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-04: 15 µl & Abs 041814: 15 µl Pct Recovery = 82% Analysis Date = 12/06/14 SpikeMix = ERA 0318-14-02: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 79% Analysis Date = 10/25/14 SpikeMix = Abs 041614: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 94% Analysis Date = 10/11/14 SpikeMix = ERA 0318-14-02: 60 µl & ERA 0319-14-04: 60 µl Pct Recovery = 82% Analysis Date = 08/28/14 SpikeMix = ERA 0319-14-04: 60 µl & ERA 0319-14-05: 60 µl Pct Recovery = 69% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 77% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 67% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 78% Analysis Date = 02/23/16 SpikeMix = Abs 052215: 40 µl & Abs 050115: 40 µl Pct Recovery = 79% Analysis Date = 07/31/15 SpikeMix = ERA 0406-15-09: 40 µl & Abs 050115: 40 µl Pct Recovery = 98% Analysis Date = 07/30/15 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 86% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-07A: 40 µl & Abs 051315: 40 µl Pct Recovery = 80% Analysis Date = 11/04/15 SpikeMix = ERA 0406-15-07A: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 77% Analysis Date = 09/10/15 SpikeMix = Abs 052215: 40 µl & ERA 0406-15-07A: 40 µl Pct Recovery = 92% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 67% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 75% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 73% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 77% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 76% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 73% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 81% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 76% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 68% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 65% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 64% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 57% Analysis Date = 11/04/14 SpikeMix = Abs 041714: 8 µl & ERA 0319-14-05: 8 µl Pct Recovery = 75% Analysis Date = 04/30/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 75% Analysis Date = 04/10/15 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 69% Analysis Date = 02/10/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 91% Analysis Date = 12/07/14 SpikeMix = ERA 0318-14-02: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 91% Analysis Date = 10/11/14 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 82% Analysis Date = 04/23/14 SpikeMix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.2: 20 µl Pct Recovery = 72% Analysis Date = 10/10/14 SpikeMix = Abs 041714: 30 µl & Abs 041814: 30 µl Pct Recovery = 90% Analysis Date = 07/20/14 SpikeMix = ERA 0318-14-02: 30 µl & Abs 041714: 30 µl Pct Recovery = 65% Analysis Date = 06/28/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 81% Analysis Date = 05/17/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 70% Analysis Date = 09/12/14 SpikeMix = Abs 041614: 30 µl & ERA 0319-14-04: 30 µl Pct Recovery = 79% Analysis Date = 08/16/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 66% Analysis Date = 07/13/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 86% Analysis Date = 11/25/15 SpikeMix = Abs 050115: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 79% Analysis Date = 11/24/15 SpikeMix = ERA 0406-15-09: 20 µl & Abs 050115: 20 µl Pct Recovery = 70% Analysis Date = 08/27/15 SpikeMix = Abs 052215: 20 µl & Abs 050115: 20 µl Pct Recovery = 74% Analysis Date = 08/11/15 SpikeMix = Abs 050115: 20 µl & Abs 051315: 20 µl Pct Recovery = 61% Analysis Date = 07/09/15 SpikeMix = Abs 050115: 20 µl & Abs 052215: 20 µl Pct Recovery = 72% Analysis Date = 06/09/15 SpikeMix = Abs 051315: 20 µl & Abs 050115: 20 µl Pct Recovery = 70% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 47% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 51% Analysis Date = 04/27/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 104% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 75% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 81% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 66% Analysis Date = 11/24/15 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 74% Analysis Date = 09/15/15 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 82% Analysis Date = 01/18/17 Pct Recovery = 76% Analysis Date = 01/13/17 Pct Recovery = 76% Analysis Date = 01/13/17 Pct Recovery = 76% Analysis Date = 01/08/17 Pct Recovery = 76% Analysis Date = 01/08/17 Pct Recovery = 76% Analysis Date = 01/03/17 Pct Recovery = 76% Analysis Date = 01/03/17 Pct Recovery = 76% Analysis Date = 12/29/16 Pct Recovery = 75% Analysis Date = 12/29/16 Pct Recovery = 75% Analysis Date = 12/24/16 Pct Recovery = 75% Analysis Date = 12/24/16 Pct Recovery = 75% Analysis Date = 12/19/16 Pct Recovery = 75% Analysis Date = 12/19/16 Pct Recovery = 75% Analysis Date = 12/14/16 Pct Recovery = 75% Analysis Date = 12/14/16 Pct Recovery = 75% Analysis Date = 12/09/16 Pct Recovery = 75% Analysis Date = 12/09/16 Pct Recovery = 75% Analysis Date = 12/04/16 Pct Recovery = 75% Analysis Date = 12/04/16 Pct Recovery = 75% Analysis Date = 11/29/16 Pct Recovery = 75% Analysis Date = 11/29/16 Pct Recovery = 75% Analysis Date = 11/24/16 Pct Recovery = 75% Analysis Date = 11/24/16 Pct Recovery = 75% Analysis Date = 11/19/16 Pct Recovery = 75% Analysis Date = 11/19/16 Pct Recovery = 75% Analysis Date = 11/14/16 Pct Recovery = 75% Analysis Date = 11/14/16 Pct Recovery = 75% Analysis Date = 11/09/16 Pct Recovery = 75% Analysis Date = 11/09/16 Pct Recovery = 75% Analysis Date = 11/04/16 Pct Recovery = 75% Analysis Date = 11/04/16 Pct Recovery = 75% Analysis Date = 10/30/16 Pct Recovery = 75% Analysis Date = 10/30/16 Pct Recovery = 75% Analysis Date = 10/25/16 Pct Recovery = 75% Analysis Date = 10/25/16 Pct Recovery = 75% Analysis Date = 10/20/16 Pct Recovery = 75% Analysis Date = 10/20/16 Pct Recovery = 75% Analysis Date = 10/15/16 Pct Recovery = 75% Analysis Date = 10/15/16 Pct Recovery = 75% Analysis Date = 10/10/16 Pct Recovery = 75% Analysis Date = 10/10/16 Pct Recovery = 75% Analysis Date = 10/05/16 Pct Recovery = 75% Analysis Date = 10/05/16 Pct Recovery = 75% Analysis Date = 09/30/16 Pct Recovery = 75% Analysis Date = 09/30/16 Pct Recovery = 75% Analysis Date = 09/25/16 Pct Recovery = 75% Analysis Date = 09/25/16 Pct Recovery = 75% Analysis Date = 09/20/16 Pct Recovery = 75% Analysis Date = 09/20/16 Pct Recovery = 75% Analysis Date = 09/15/16 Pct Recovery = 75% Analysis Date = 09/15/16 Pct Recovery = 75% Analysis Date = 09/10/16 Pct Recovery = 75% Analysis Date = 09/10/16 Pct Recovery = 75% Analysis Date = 09/05/16 Pct Recovery = 74% Analysis Date = 09/05/16 Pct Recovery = 74% Analysis Date = 08/31/16 Pct Recovery = 74% Analysis Date = 08/31/16 Pct Recovery = 74% Analysis Date = 08/26/16 Pct Recovery = 74% Analysis Date = 08/26/16 Pct Recovery = 74% Analysis Date = 08/21/16 Pct Recovery = 74% Analysis Date = 08/21/16 Pct Recovery = 74% Analysis Date = 08/16/16 Pct Recovery = 74% Analysis Date = 08/16/16 Pct Recovery = 74% Analysis Date = 08/11/16 Pct Recovery = 74% Analysis Date = 08/11/16 Pct Recovery = 74% Analysis Date = 08/06/16 Pct Recovery = 74% Analysis Date = 08/06/16 Pct Recovery = 74% Analysis Date = 08/01/16 Pct Recovery = 74% Analysis Date = 08/01/16 Pct Recovery = 74% Analysis Date = 07/27/16 Pct Recovery = 74% Analysis Date = 07/27/16 Pct Recovery = 74% Analysis Date = 07/22/16 Pct Recovery = 74% Analysis Date = 07/22/16 Pct Recovery = 74% Analysis Date = 07/17/16 Pct Recovery = 74% Analysis Date = 07/17/16 Pct Recovery = 74% Analysis Date = 07/12/16 Pct Recovery = 74% Analysis Date = 07/12/16 Pct Recovery = 74% Analysis Date = 07/07/16 Pct Recovery = 74% Analysis Date = 07/07/16 Pct Recovery = 74% Analysis Date = 07/02/16 Pct Recovery = 74% Analysis Date = 07/02/16 Pct Recovery = 74% Analysis Date = 06/27/16 Pct Recovery = 74% Analysis Date = 06/27/16 Pct Recovery = 74% Analysis Date = 06/22/16 Pct Recovery = 74% Analysis Date = 06/22/16 Pct Recovery = 74% Analysis Date = 06/17/16 Pct Recovery = 74% Analysis Date = 06/17/16 Pct Recovery = 74% Analysis Date = 06/12/16 Pct Recovery = 74% Analysis Date = 06/12/16 Pct Recovery = 74% Analysis Date = 06/07/16 Pct Recovery = 74% Analysis Date = 06/07/16 Pct Recovery = 74% Analysis Date = 06/02/16 Pct Recovery = 74% Analysis Date = 06/02/16 Pct Recovery = 74% Analysis Date = 05/28/16 Pct Recovery = 74% Analysis Date = 05/28/16 Pct Recovery = 74% Analysis Date = 05/23/16 Pct Recovery = 74% Analysis Date = 05/23/16 Pct Recovery = 74% Analysis Date = 05/18/16 Pct Recovery = 74% Analysis Date = 05/18/16 Pct Recovery = 74% Analysis Date = 05/13/16 Pct Recovery = 74% Analysis Date = 05/13/16 Pct Recovery = 74% Analysis Date = 05/08/16 Pct Recovery = 74% Analysis Date = 05/08/16 Pct Recovery = 74% Analysis Date = 05/03/16 Pct Recovery = 74% Analysis Date = 05/03/16 Pct Recovery = 74% Analysis Date = 04/28/16 Pct Recovery = 74% Analysis Date = 04/28/16 Pct Recovery = 74% Analysis Date = 04/23/16 Pct Recovery = 74% Analysis Date = 04/23/16 Pct Recovery = 74% Analysis Date = 04/18/16 Pct Recovery = 74% Analysis Date = 04/18/16 Pct Recovery = 74% Analysis Date = 04/13/16 Pct Recovery = 74% Analysis Date = 04/13/16 Pct Recovery = 74% Analysis Date = 04/08/16 Pct Recovery = 74% Analysis Date = 04/08/16 Pct Recovery = 74% Analysis Date = 04/03/16 Pct Recovery = 75% Analysis Date = 04/03/16 Pct Recovery = 75% Analysis Date = 03/29/16 Pct Recovery = 75% Analysis Date = 03/29/16 Pct Recovery = 75% Analysis Date = 03/24/16 Pct Recovery = 75% Analysis Date = 03/24/16 Pct Recovery = 75% Analysis Date = 03/19/16 Pct Recovery = 75% Analysis Date = 03/19/16 Pct Recovery = 75% Analysis Date = 03/14/16 Pct Recovery = 75% Analysis Date = 03/14/16 Pct Recovery = 75% Analysis Date = 03/09/16 Pct Recovery = 75% Analysis Date = 03/09/16 Pct Recovery = 75% Analysis Date = 03/04/16 Pct Recovery = 75% Analysis Date = 03/04/16 Pct Recovery = 75% Analysis Date = 02/28/16 Pct Recovery = 75% Analysis Date = 02/28/16 Pct Recovery = 75% Analysis Date = 02/23/16 Pct Recovery = 75% Analysis Date = 02/23/16 Pct Recovery = 75% Analysis Date = 02/18/16 Pct Recovery = 76% Analysis Date = 02/18/16 Pct Recovery = 76% Analysis Date = 02/13/16 Pct Recovery = 76% Analysis Date = 02/13/16 Pct Recovery = 76% Analysis Date = 02/08/16 Pct Recovery = 76% Analysis Date = 02/08/16 Pct Recovery = 76% Analysis Date = 02/03/16 Pct Recovery = 76% Analysis Date = 02/03/16 Pct Recovery = 76% Analysis Date = 01/29/16 Pct Recovery = 76% Analysis Date = 01/29/16 Pct Recovery = 76% Analysis Date = 01/24/16 Pct Recovery = 76% Analysis Date = 01/24/16 Pct Recovery = 76% Analysis Date = 01/19/16 Pct Recovery = 76% Analysis Date = 01/19/16 Pct Recovery = 76% Analysis Date = 01/14/16 Pct Recovery = 76% Analysis Date = 01/14/16 Pct Recovery = 76% Analysis Date = 01/09/16 Pct Recovery = 77% Analysis Date = 01/09/16 Pct Recovery = 77% Analysis Date = 01/04/16 Pct Recovery = 77% Analysis Date = 01/04/16 Pct Recovery = 77% Analysis Date = 12/30/15 Pct Recovery = 77% Analysis Date = 12/30/15 Pct Recovery = 77% Analysis Date = 12/25/15 Pct Recovery = 77% Analysis Date = 12/25/15 Pct Recovery = 77% Analysis Date = 12/20/15 Pct Recovery = 77% Analysis Date = 12/20/15 Pct Recovery = 77% Analysis Date = 12/15/15 Pct Recovery = 77% Analysis Date = 12/15/15 Pct Recovery = 77% Analysis Date = 12/10/15 Pct Recovery = 77% Analysis Date = 12/10/15 Pct Recovery = 77% Analysis Date = 12/05/15 Pct Recovery = 77% Analysis Date = 12/05/15 Pct Recovery = 77% Analysis Date = 11/30/15 Pct Recovery = 78% Analysis Date = 11/30/15 Pct Recovery = 78% Analysis Date = 11/25/15 Pct Recovery = 78% Analysis Date = 11/25/15 Pct Recovery = 78% Analysis Date = 11/20/15 Pct Recovery = 78% Analysis Date = 11/20/15 Pct Recovery = 78% Analysis Date = 11/15/15 Pct Recovery = 78% Analysis Date = 11/15/15 Pct Recovery = 78% Analysis Date = 11/10/15 Pct Recovery = 78% Analysis Date = 11/10/15 Pct Recovery = 78% Analysis Date = 11/05/15 Pct Recovery = 78% Analysis Date = 11/05/15 Pct Recovery = 78% Analysis Date = 10/31/15 Pct Recovery = 78% Analysis Date = 10/31/15 Pct Recovery = 78% Analysis Date = 10/26/15 Pct Recovery = 78% Analysis Date = 10/26/15 Pct Recovery = 78% Analysis Date = 10/21/15 Pct Recovery = 79% Analysis Date = 10/21/15 Pct Recovery = 79% Analysis Date = 10/16/15 Pct Recovery = 79% Analysis Date = 10/16/15 Pct Recovery = 79% Analysis Date = 10/11/15 Pct Recovery = 79% Analysis Date = 10/11/15 Pct Recovery = 79% Analysis Date = 10/06/15 Pct Recovery = 79% Analysis Date = 10/06/15 Pct Recovery = 79% Analysis Date = 10/01/15 Pct Recovery = 79% Analysis Date = 10/01/15 Pct Recovery = 79% Analysis Date = 09/26/15 Pct Recovery = 79% Analysis Date = 09/26/15 Pct Recovery = 79% Analysis Date = 09/21/15 Pct Recovery = 79% Analysis Date = 09/21/15 Pct Recovery = 79% Analysis Date = 09/16/15 Pct Recovery = 79% Analysis Date = 09/16/15 Pct Recovery = 79% Analysis Date = 09/11/15 Pct Recovery = 79% Analysis Date = 09/11/15 Pct Recovery = 79% Analysis Date = 09/05/15 Pct Recovery = 80% Analysis Date = 09/05/15 Pct Recovery = 80% Analysis Date = 08/31/15 Pct Recovery = 80% Analysis Date = 08/31/15 Pct Recovery = 80% Analysis Date = 08/26/15 Pct Recovery = 80% Analysis Date = 08/26/15 Pct Recovery = 80% Analysis Date = 08/21/15 Pct Recovery = 80% Analysis Date = 08/21/15 Pct Recovery = 80% Analysis Date = 08/16/15 Pct Recovery = 80% Analysis Date = 08/16/15 Pct Recovery = 80% Analysis Date = 08/11/15 Pct Recovery = 80% Analysis Date = 08/11/15 Pct Recovery = 80% Analysis Date = 08/06/15 Pct Recovery = 80% Analysis Date = 08/06/15 Pct Recovery = 80% Analysis Date = 08/01/15 Pct Recovery = 80% Analysis Date = 08/01/15 Pct Recovery = 80% Analysis Date = 07/27/15 Pct Recovery = 81% Analysis Date = 07/27/15 Pct Recovery = 81% Analysis Date = 07/22/15 Pct Recovery = 81% Analysis Date = 07/22/15 Pct Recovery = 81% Analysis Date = 07/17/15 Pct Recovery = 81% Analysis Date = 07/17/15 Pct Recovery = 81% Analysis Date = 07/12/15 Pct Recovery = 81% Analysis Date = 07/12/15 Pct Recovery = 81% Analysis Date = 07/07/15 Pct Recovery = 81% Analysis Date = 07/07/15 Pct Recovery = 81% Analysis Date = 07/02/15 Pct Recovery = 81% Analysis Date = 07/02/15 Pct Recovery = 81% Analysis Date = 06/27/15 Pct Recovery = 81% Analysis Date = 06/27/15 Pct Recovery = 81% Analysis Date = 06/22/15 Pct Recovery = 81% Analysis Date = 06/22/15 Pct Recovery = 81% Analysis Date = 06/17/15 Pct Recovery = 81% Analysis Date = 06/17/15 Pct Recovery = 81% Analysis Date = 06/12/15 Pct Recovery = 81% Analysis Date = 06/12/15 Pct Recovery = 81% Analysis Date = 06/07/15 Pct Recovery = 81% Analysis Date = 06/07/15 Pct Recovery = 81% Analysis Date = 06/02/15 Pct Recovery = 81% Analysis Date = 06/02/15 Pct Recovery = 81% Analysis Date = 05/28/15 Pct Recovery = 81% Analysis Date = 05/28/15 Pct Recovery = 81% Analysis Date = 05/23/15 Pct Recovery = 81% Analysis Date = 05/23/15 Pct Recovery = 81% Analysis Date = 05/18/15 Pct Recovery = 81% Analysis Date = 05/18/15 Pct Recovery = 81% Analysis Date = 05/13/15 Pct Recovery = 81% Analysis Date = 05/13/15 Pct Recovery = 81% Analysis Date = 05/08/15 Pct Recovery = 81% Analysis Date = 05/08/15 Pct Recovery = 81% Analysis Date = 05/03/15 Pct Recovery = 81% Analysis Date = 05/03/15 Pct Recovery = 81% Analysis Date = 04/28/15 Pct Recovery = 81% Analysis Date = 04/28/15 Pct Recovery = 81% Analysis Date = 04/23/15 Pct Recovery = 81% Analysis Date = 04/23/15 Pct Recovery = 81% Analysis Date = 04/18/15 Pct Recovery = 82% Analysis Date = 04/18/15 Pct Recovery = 82% Analysis Date = 04/13/15 Pct Recovery = 82% Analysis Date = 04/13/15 Pct Recovery = 82% Analysis Date = 04/08/15 Pct Recovery = 82% Analysis Date = 04/08/15 Pct Recovery = 82% Analysis Date = 04/03/15 Pct Recovery = 82% Analysis Date = 04/03/15 Pct Recovery = 82% Analysis Date = 03/29/15 Pct Recovery = 82% Analysis Date = 03/29/15 Pct Recovery = 82% Analysis Date = 03/24/15 Pct Recovery = 82% Analysis Date = 03/24/15 Pct Recovery = 82% Analysis Date = 03/19/15 Pct Recovery = 81% Analysis Date = 03/19/15 Pct Recovery = 81% Analysis Date = 03/14/15 Pct Recovery = 81% Analysis Date = 03/14/15 Pct Recovery = 81% Analysis Date = 03/09/15 Pct Recovery = 81% Analysis Date = 03/09/15 Pct Recovery = 81% Analysis Date = 03/04/15 Pct Recovery = 81% Analysis Date = 03/04/15 Pct Recovery = 81% Analysis Date = 02/27/15 Pct Recovery = 81% Analysis Date = 02/27/15 Pct Recovery = 81% Analysis Date = 02/22/15 Pct Recovery = 81% Analysis Date = 02/22/15 Pct Recovery = 81% Analysis Date = 02/17/15 Pct Recovery = 81% Analysis Date = 02/17/15 Pct Recovery = 81% Analysis Date = 02/12/15 Pct Recovery = 81% Analysis Date = 02/12/15 Pct Recovery = 81% Analysis Date = 02/07/15 Pct Recovery = 81% Analysis Date = 02/07/15 Pct Recovery = 81% Analysis Date = 02/02/15 Pct Recovery = 81% Analysis Date = 02/02/15 Pct Recovery = 81% Analysis Date = 01/28/15 Pct Recovery = 81% Analysis Date = 01/28/15 Pct Recovery = 81% Analysis Date = 01/23/15 Pct Recovery = 81% Analysis Date = 01/23/15 Pct Recovery = 81% Analysis Date = 01/18/15 Pct Recovery = 81% Analysis Date = 01/18/15 Pct Recovery = 81% Analysis Date = 01/13/15 Pct Recovery = 81% Analysis Date = 01/13/15 Pct Recovery = 81% Analysis Date = 01/08/15 Pct Recovery = 81% Analysis Date = 01/08/15 Pct Recovery = 81% Analysis Date = 01/03/15 Pct Recovery = 81% Analysis Date = 01/03/15 Pct Recovery = 81% Analysis Date = 12/29/14 Pct Recovery = 81% Analysis Date = 12/29/14 Pct Recovery = 81% Analysis Date = 12/24/14 Pct Recovery = 81% Analysis Date = 12/24/14 Pct Recovery = 81% Analysis Date = 12/19/14 Pct Recovery = 81% Analysis Date = 12/19/14 Pct Recovery = 81% Analysis Date = 12/14/14 Pct Recovery = 81% Analysis Date = 12/14/14 Pct Recovery = 81% Analysis Date = 12/09/14 Pct Recovery = 81% Analysis Date = 12/09/14 Pct Recovery = 81% Analysis Date = 12/04/14 Pct Recovery = 81% Analysis Date = 12/04/14 Pct Recovery = 81% Analysis Date = 11/29/14 Pct Recovery = 81% Analysis Date = 11/29/14 Pct Recovery = 81% Analysis Date = 11/24/14 Pct Recovery = 81% Analysis Date = 11/24/14 Pct Recovery = 81% Analysis Date = 11/19/14 Pct Recovery = 81% Analysis Date = 11/19/14 Pct Recovery = 81% Analysis Date = 11/14/14 Pct Recovery = 80% Analysis Date = 11/14/14 Pct Recovery = 80% Analysis Date = 11/09/14 Pct Recovery = 80% Analysis Date = 11/09/14 Pct Recovery = 80% Analysis Date = 11/04/14 Pct Recovery = 80% Analysis Date = 11/04/14 Pct Recovery = 80% Analysis Date = 10/30/14 Pct Recovery = 80% Analysis Date = 10/30/14 Pct Recovery = 80% Analysis Date = 10/25/14 Pct Recovery = 80% Analysis Date = 10/25/14 Pct Recovery = 80% Analysis Date = 10/20/14 Pct Recovery = 80% Analysis Date = 10/20/14 Pct Recovery = 80% Analysis Date = 10/15/14 Pct Recovery = 80% Analysis Date = 10/15/14 Pct Recovery = 80% Analysis Date = 10/10/14 Pct Recovery = 80% Analysis Date = 10/10/14 Pct Recovery = 80% Analysis Date = 10/05/14 Pct Recovery = 80% Analysis Date = 10/05/14 Pct Recovery = 80% Analysis Date = 09/30/14 Pct Recovery = 80% Analysis Date = 09/30/14 Pct Recovery = 80% Analysis Date = 09/25/14 Pct Recovery = 80% Analysis Date = 09/25/14 Pct Recovery = 80% Analysis Date = 09/20/14 Pct Recovery = 80% Analysis Date = 09/20/14 Pct Recovery = 80% Analysis Date = 09/15/14 Pct Recovery = 80% Analysis Date = 09/15/14 Pct Recovery = 80% Analysis Date = 09/10/14 Pct Recovery = 80% Analysis Date = 09/10/14 Pct Recovery = 80% Analysis Date = 09/05/14 Pct Recovery = 80% Analysis Date = 09/05/14 Pct Recovery = 80% Analysis Date = 08/31/14 Pct Recovery = 80% Analysis Date = 08/31/14 Pct Recovery = 80% Analysis Date = 08/26/14 Pct Recovery = 80% Analysis Date = 08/26/14 Pct Recovery = 80% Analysis Date = 08/21/14 Pct Recovery = 80% Analysis Date = 08/21/14 Pct Recovery = 80% Analysis Date = 08/16/14 Pct Recovery = 80% Analysis Date = 08/16/14 Pct Recovery = 80% Analysis Date = 08/11/14 Pct Recovery = 80% Analysis Date = 08/11/14 Pct Recovery = 80% Analysis Date = 08/06/14 Pct Recovery = 80% Analysis Date = 08/06/14 Pct Recovery = 80% Analysis Date = 08/01/14 Pct Recovery = 80% Analysis Date = 08/01/14 Pct Recovery = 80% Analysis Date = 07/27/14 Pct Recovery = 79% Analysis Date = 07/27/14 Pct Recovery = 79% Analysis Date = 07/22/14 Pct Recovery = 79% Analysis Date = 07/22/14 Pct Recovery = 79% Analysis Date = 07/17/14 Pct Recovery = 79% Analysis Date = 07/17/14 Pct Recovery = 79% Analysis Date = 07/12/14 Pct Recovery = 79% Analysis Date = 07/12/14 Pct Recovery = 79% Analysis Date = 07/07/14 Pct Recovery = 79% Analysis Date = 07/07/14 Pct Recovery = 79% Analysis Date = 07/02/14 Pct Recovery = 79% Analysis Date = 07/02/14 Pct Recovery = 79% Analysis Date = 06/27/14 Pct Recovery = 79% Analysis Date = 06/27/14 Pct Recovery = 79% Analysis Date = 06/22/14 Pct Recovery = 79% Analysis Date = 06/22/14 Pct Recovery = 79% Analysis Date = 06/17/14 Pct Recovery = 79% Analysis Date = 06/17/14 Pct Recovery = 79% Analysis Date = 06/12/14 Pct Recovery = 79% Analysis Date = 06/12/14 Pct Recovery = 79% Analysis Date = 06/07/14 Pct Recovery = 79% Analysis Date = 06/07/14 Pct Recovery = 79% Analysis Date = 06/02/14 Pct Recovery = 79% Analysis Date = 06/02/14 Pct Recovery = 79% Analysis Date = 05/28/14 Pct Recovery = 79% Analysis Date = 05/28/14 Pct Recovery = 79% Analysis Date = 05/23/14 Pct Recovery = 79% Analysis Date = 05/23/14 Pct Recovery = 79% Analysis Date = 05/18/14 Pct Recovery = 79% Analysis Date = 05/18/14 Pct Recovery = 79% Analysis Date = 05/13/14 Pct Recovery = 79% Analysis Date = 05/13/14 Pct Recovery = 79% Analysis Date = 05/08/14 Pct Recovery = 79% Analysis Date = 05/08/14 Pct Recovery = 79% Analysis Date = 05/03/14 Pct Recovery = 78% Analysis Date = 05/03/14 Pct Recovery = 78% Analysis Date = 04/28/14 Pct Recovery = 78% Analysis Date = 04/28/14 Pct Recovery = 78% Analysis Date = 04/23/14 Pct Recovery = 78% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
SULFAMETHIZOLE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 78 78% 11% 77% 8%
Total 78 78% 11% 77% 8%

Sample Statistics
SULFAMETHIZOLE

Characteristic N % % Basis
Plotted 78 99% Spiked
Estimated Values 5 6% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 79 .  
False Negatives 1 1% 1 out of 79
Not Spiked 36 .  
False Positives 0 0% 0 out of 36

BQS OBSP Determination:
SULFAMETHOXAZOLE
METHOD: 2440 , TESTIDCODE: 67454LCM56
Open Data Set

Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 83% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 87% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 99% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 93% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 80 µl & ERA 0406-15-08: 80 µl Pct Recovery = 78% Analysis Date = 11/05/15 SpikeMix = ERA 0406-15-08: 80 µl & Abs 052215: 80 µl Pct Recovery = 82% Analysis Date = 11/24/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 90% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 80 µl & Abs 051315: 80 µl Pct Recovery = 90% Analysis Date = 10/01/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 92% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 70% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 74% Analysis Date = 09/24/16 SpikeMix = Crescent EN160610015: 80 µl & Abs 061416: 80 µl Pct Recovery = 83% Analysis Date = 09/24/16 SpikeMix = Abs 061416: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 74% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 72% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 77% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 86% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 81% Analysis Date = 04/29/15 SpikeMix = ERA 0319-14-05: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 96% Analysis Date = 03/11/15 SpikeMix = ERA 0318-14-02: 15 µl & Abs 041714: 15 µl Pct Recovery = 79% Analysis Date = 02/06/15 SpikeMix = Abs 041814: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 87% Analysis Date = 12/06/14 SpikeMix = ERA 0318-14-02: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 107% Analysis Date = 10/11/14 SpikeMix = ERA 0318-14-02: 60 µl & ERA 0319-14-04: 60 µl Pct Recovery = 83% Analysis Date = 08/21/14 SpikeMix = ERA 0318-14-02: 60 µl & Abs 041714: 60 µl Pct Recovery = 75% Analysis Date = 07/26/14 SpikeMix = ERA 0319-14-05: 60 µl & ERA 0318-14-02: 60 µl Pct Recovery = 105% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 89% Analysis Date = 12/07/14 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 78% Analysis Date = 10/25/14 SpikeMix = Abs 041614: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 84% Analysis Date = 06/22/14 SpikeMix = Abs 041814: 60 µl & Abs 041614: 60 µl Pct Recovery = 121% Analysis Date = 06/11/14 SpikeMix = Abs 041614: 60 µl & Abs 041714: 60 µl Pct Recovery = 79% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-08: 40 µl & Abs 052215: 40 µl Pct Recovery = 109% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 86% Analysis Date = 11/04/15 SpikeMix = ERA 0406-15-07A: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 80% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-08: 40 µl & ERA 0406-15-09: 40 µl Pct Recovery = 86% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 65% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 59% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-07A: 40 µl & Abs 051315: 40 µl Pct Recovery = 70% Analysis Date = 07/31/15 SpikeMix = Abs 051315: 40 µl & Abs 052215: 40 µl Pct Recovery = 90% Analysis Date = 07/30/15 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 96% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 68% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 87% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 78% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 78% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 74% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 74% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 77% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 71% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 76% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 81% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 61% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 68% Analysis Date = 12/07/14 SpikeMix = ERA 0318-14-02: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 84% Analysis Date = 11/04/14 SpikeMix = Abs 041814: 8 µl & ERA 0318-14-02: 8 µl Pct Recovery = 81% Analysis Date = 04/30/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 84% Analysis Date = 02/10/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 84% Analysis Date = 10/24/14 SpikeMix = ERA 0319-14-05: 8 µl & Abs 041614: 8 µl Pct Recovery = 70% Analysis Date = 10/10/14 SpikeMix = Abs 041814: 30 µl & ERA 0318-14-02: 30 µl Pct Recovery = 108% Analysis Date = 08/30/14 SpikeMix = ERA 0318-14-02: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 41% Analysis Date = 07/20/14 SpikeMix = ERA 0318-14-02: 30 µl & Abs 041714: 30 µl Pct Recovery = 61% Analysis Date = 09/12/14 SpikeMix = Abs 041614: 30 µl & ERA 0319-14-04: 30 µl Pct Recovery = 75% Analysis Date = 07/13/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 54% Analysis Date = 06/28/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 66% Analysis Date = 05/30/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 75% Analysis Date = 05/17/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 84% Analysis Date = 04/27/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 83% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 81% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-08: 20 µl & ERA 0406-15-09: 20 µl Pct Recovery = 80% Analysis Date = 11/25/15 SpikeMix = Abs 050115: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 84% Analysis Date = 09/15/15 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 74% Analysis Date = 09/09/15 SpikeMix = ERA 0406-15-08: 20 µl & Abs 052215: 20 µl Pct Recovery = 95% Analysis Date = 02/23/16 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 83% Analysis Date = 08/11/15 SpikeMix = Abs 050115: 20 µl & Abs 051315: 20 µl Pct Recovery = 48% Analysis Date = 06/26/15 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 83% Analysis Date = 06/09/15 SpikeMix = Abs 051315: 20 µl & Abs 050115: 20 µl Pct Recovery = 68% Analysis Date = 04/09/16 SpikeMix = Abs 051315: 10 µl & ERA 0406-15-09: 10 µl Pct Recovery = 63% Analysis Date = 01/18/17 Pct Recovery = 80% Analysis Date = 01/14/17 Pct Recovery = 80% Analysis Date = 01/14/17 Pct Recovery = 80% Analysis Date = 01/09/17 Pct Recovery = 80% Analysis Date = 01/09/17 Pct Recovery = 80% Analysis Date = 01/04/17 Pct Recovery = 80% Analysis Date = 01/04/17 Pct Recovery = 80% Analysis Date = 12/30/16 Pct Recovery = 80% Analysis Date = 12/30/16 Pct Recovery = 80% Analysis Date = 12/25/16 Pct Recovery = 80% Analysis Date = 12/25/16 Pct Recovery = 80% Analysis Date = 12/20/16 Pct Recovery = 80% Analysis Date = 12/20/16 Pct Recovery = 80% Analysis Date = 12/15/16 Pct Recovery = 80% Analysis Date = 12/15/16 Pct Recovery = 80% Analysis Date = 12/10/16 Pct Recovery = 79% Analysis Date = 12/10/16 Pct Recovery = 79% Analysis Date = 12/05/16 Pct Recovery = 79% Analysis Date = 12/05/16 Pct Recovery = 79% Analysis Date = 12/01/16 Pct Recovery = 79% Analysis Date = 12/01/16 Pct Recovery = 79% Analysis Date = 11/26/16 Pct Recovery = 79% Analysis Date = 11/26/16 Pct Recovery = 79% Analysis Date = 11/21/16 Pct Recovery = 79% Analysis Date = 11/21/16 Pct Recovery = 79% Analysis Date = 11/16/16 Pct Recovery = 79% Analysis Date = 11/16/16 Pct Recovery = 79% Analysis Date = 11/11/16 Pct Recovery = 79% Analysis Date = 11/11/16 Pct Recovery = 79% Analysis Date = 11/06/16 Pct Recovery = 79% Analysis Date = 11/06/16 Pct Recovery = 79% Analysis Date = 11/01/16 Pct Recovery = 79% Analysis Date = 11/01/16 Pct Recovery = 79% Analysis Date = 10/27/16 Pct Recovery = 79% Analysis Date = 10/27/16 Pct Recovery = 79% Analysis Date = 10/22/16 Pct Recovery = 78% Analysis Date = 10/22/16 Pct Recovery = 78% Analysis Date = 10/18/16 Pct Recovery = 78% Analysis Date = 10/18/16 Pct Recovery = 78% Analysis Date = 10/13/16 Pct Recovery = 78% Analysis Date = 10/13/16 Pct Recovery = 78% Analysis Date = 10/08/16 Pct Recovery = 78% Analysis Date = 10/08/16 Pct Recovery = 78% Analysis Date = 10/03/16 Pct Recovery = 78% Analysis Date = 10/03/16 Pct Recovery = 78% Analysis Date = 09/28/16 Pct Recovery = 78% Analysis Date = 09/28/16 Pct Recovery = 78% Analysis Date = 09/23/16 Pct Recovery = 78% Analysis Date = 09/23/16 Pct Recovery = 78% Analysis Date = 09/18/16 Pct Recovery = 78% Analysis Date = 09/18/16 Pct Recovery = 78% Analysis Date = 09/13/16 Pct Recovery = 78% Analysis Date = 09/13/16 Pct Recovery = 78% Analysis Date = 09/08/16 Pct Recovery = 78% Analysis Date = 09/08/16 Pct Recovery = 78% Analysis Date = 09/04/16 Pct Recovery = 78% Analysis Date = 09/04/16 Pct Recovery = 78% Analysis Date = 08/30/16 Pct Recovery = 78% Analysis Date = 08/30/16 Pct Recovery = 78% Analysis Date = 08/25/16 Pct Recovery = 78% Analysis Date = 08/25/16 Pct Recovery = 78% Analysis Date = 08/20/16 Pct Recovery = 78% Analysis Date = 08/20/16 Pct Recovery = 78% Analysis Date = 08/15/16 Pct Recovery = 78% Analysis Date = 08/15/16 Pct Recovery = 78% Analysis Date = 08/10/16 Pct Recovery = 78% Analysis Date = 08/10/16 Pct Recovery = 78% Analysis Date = 08/05/16 Pct Recovery = 78% Analysis Date = 08/05/16 Pct Recovery = 78% Analysis Date = 07/31/16 Pct Recovery = 77% Analysis Date = 07/31/16 Pct Recovery = 77% Analysis Date = 07/26/16 Pct Recovery = 77% Analysis Date = 07/26/16 Pct Recovery = 77% Analysis Date = 07/22/16 Pct Recovery = 77% Analysis Date = 07/22/16 Pct Recovery = 77% Analysis Date = 07/17/16 Pct Recovery = 77% Analysis Date = 07/17/16 Pct Recovery = 77% Analysis Date = 07/12/16 Pct Recovery = 78% Analysis Date = 07/12/16 Pct Recovery = 78% Analysis Date = 07/07/16 Pct Recovery = 78% Analysis Date = 07/07/16 Pct Recovery = 78% Analysis Date = 07/02/16 Pct Recovery = 78% Analysis Date = 07/02/16 Pct Recovery = 78% Analysis Date = 06/27/16 Pct Recovery = 78% Analysis Date = 06/27/16 Pct Recovery = 78% Analysis Date = 06/22/16 Pct Recovery = 78% Analysis Date = 06/22/16 Pct Recovery = 78% Analysis Date = 06/17/16 Pct Recovery = 78% Analysis Date = 06/17/16 Pct Recovery = 78% Analysis Date = 06/12/16 Pct Recovery = 78% Analysis Date = 06/12/16 Pct Recovery = 78% Analysis Date = 06/08/16 Pct Recovery = 78% Analysis Date = 06/08/16 Pct Recovery = 78% Analysis Date = 06/03/16 Pct Recovery = 78% Analysis Date = 06/03/16 Pct Recovery = 78% Analysis Date = 05/29/16 Pct Recovery = 78% Analysis Date = 05/29/16 Pct Recovery = 78% Analysis Date = 05/24/16 Pct Recovery = 78% Analysis Date = 05/24/16 Pct Recovery = 78% Analysis Date = 05/19/16 Pct Recovery = 78% Analysis Date = 05/19/16 Pct Recovery = 78% Analysis Date = 05/14/16 Pct Recovery = 78% Analysis Date = 05/14/16 Pct Recovery = 78% Analysis Date = 05/09/16 Pct Recovery = 78% Analysis Date = 05/09/16 Pct Recovery = 78% Analysis Date = 05/04/16 Pct Recovery = 78% Analysis Date = 05/04/16 Pct Recovery = 78% Analysis Date = 04/29/16 Pct Recovery = 78% Analysis Date = 04/29/16 Pct Recovery = 78% Analysis Date = 04/25/16 Pct Recovery = 79% Analysis Date = 04/25/16 Pct Recovery = 79% Analysis Date = 04/20/16 Pct Recovery = 79% Analysis Date = 04/20/16 Pct Recovery = 79% Analysis Date = 04/15/16 Pct Recovery = 79% Analysis Date = 04/15/16 Pct Recovery = 79% Analysis Date = 04/10/16 Pct Recovery = 79% Analysis Date = 04/10/16 Pct Recovery = 79% Analysis Date = 04/05/16 Pct Recovery = 79% Analysis Date = 04/05/16 Pct Recovery = 79% Analysis Date = 03/31/16 Pct Recovery = 79% Analysis Date = 03/31/16 Pct Recovery = 79% Analysis Date = 03/26/16 Pct Recovery = 79% Analysis Date = 03/26/16 Pct Recovery = 79% Analysis Date = 03/21/16 Pct Recovery = 79% Analysis Date = 03/21/16 Pct Recovery = 79% Analysis Date = 03/16/16 Pct Recovery = 79% Analysis Date = 03/16/16 Pct Recovery = 79% Analysis Date = 03/12/16 Pct Recovery = 79% Analysis Date = 03/12/16 Pct Recovery = 79% Analysis Date = 03/07/16 Pct Recovery = 79% Analysis Date = 03/07/16 Pct Recovery = 79% Analysis Date = 03/02/16 Pct Recovery = 80% Analysis Date = 03/02/16 Pct Recovery = 80% Analysis Date = 02/26/16 Pct Recovery = 80% Analysis Date = 02/26/16 Pct Recovery = 80% Analysis Date = 02/21/16 Pct Recovery = 80% Analysis Date = 02/21/16 Pct Recovery = 80% Analysis Date = 02/16/16 Pct Recovery = 80% Analysis Date = 02/16/16 Pct Recovery = 80% Analysis Date = 02/11/16 Pct Recovery = 80% Analysis Date = 02/11/16 Pct Recovery = 80% Analysis Date = 02/06/16 Pct Recovery = 80% Analysis Date = 02/06/16 Pct Recovery = 80% Analysis Date = 02/01/16 Pct Recovery = 80% Analysis Date = 02/01/16 Pct Recovery = 80% Analysis Date = 01/28/16 Pct Recovery = 80% Analysis Date = 01/28/16 Pct Recovery = 80% Analysis Date = 01/23/16 Pct Recovery = 80% Analysis Date = 01/23/16 Pct Recovery = 80% Analysis Date = 01/18/16 Pct Recovery = 80% Analysis Date = 01/18/16 Pct Recovery = 80% Analysis Date = 01/13/16 Pct Recovery = 81% Analysis Date = 01/13/16 Pct Recovery = 81% Analysis Date = 01/08/16 Pct Recovery = 81% Analysis Date = 01/08/16 Pct Recovery = 81% Analysis Date = 01/03/16 Pct Recovery = 81% Analysis Date = 01/03/16 Pct Recovery = 81% Analysis Date = 12/29/15 Pct Recovery = 81% Analysis Date = 12/29/15 Pct Recovery = 81% Analysis Date = 12/24/15 Pct Recovery = 81% Analysis Date = 12/24/15 Pct Recovery = 81% Analysis Date = 12/19/15 Pct Recovery = 81% Analysis Date = 12/19/15 Pct Recovery = 81% Analysis Date = 12/15/15 Pct Recovery = 81% Analysis Date = 12/15/15 Pct Recovery = 81% Analysis Date = 12/10/15 Pct Recovery = 81% Analysis Date = 12/10/15 Pct Recovery = 81% Analysis Date = 12/05/15 Pct Recovery = 81% Analysis Date = 12/05/15 Pct Recovery = 81% Analysis Date = 11/30/15 Pct Recovery = 81% Analysis Date = 11/30/15 Pct Recovery = 81% Analysis Date = 11/25/15 Pct Recovery = 81% Analysis Date = 11/25/15 Pct Recovery = 81% Analysis Date = 11/20/15 Pct Recovery = 82% Analysis Date = 11/20/15 Pct Recovery = 82% Analysis Date = 11/15/15 Pct Recovery = 82% Analysis Date = 11/15/15 Pct Recovery = 82% Analysis Date = 11/10/15 Pct Recovery = 82% Analysis Date = 11/10/15 Pct Recovery = 82% Analysis Date = 11/05/15 Pct Recovery = 82% Analysis Date = 11/05/15 Pct Recovery = 82% Analysis Date = 11/01/15 Pct Recovery = 82% Analysis Date = 11/01/15 Pct Recovery = 82% Analysis Date = 10/27/15 Pct Recovery = 82% Analysis Date = 10/27/15 Pct Recovery = 82% Analysis Date = 10/22/15 Pct Recovery = 82% Analysis Date = 10/22/15 Pct Recovery = 82% Analysis Date = 10/17/15 Pct Recovery = 82% Analysis Date = 10/17/15 Pct Recovery = 82% Analysis Date = 10/12/15 Pct Recovery = 82% Analysis Date = 10/12/15 Pct Recovery = 82% Analysis Date = 10/07/15 Pct Recovery = 82% Analysis Date = 10/07/15 Pct Recovery = 82% Analysis Date = 10/02/15 Pct Recovery = 82% Analysis Date = 10/02/15 Pct Recovery = 82% Analysis Date = 09/27/15 Pct Recovery = 82% Analysis Date = 09/27/15 Pct Recovery = 82% Analysis Date = 09/22/15 Pct Recovery = 83% Analysis Date = 09/22/15 Pct Recovery = 83% Analysis Date = 09/17/15 Pct Recovery = 83% Analysis Date = 09/17/15 Pct Recovery = 83% Analysis Date = 09/13/15 Pct Recovery = 83% Analysis Date = 09/13/15 Pct Recovery = 83% Analysis Date = 09/08/15 Pct Recovery = 83% Analysis Date = 09/08/15 Pct Recovery = 83% Analysis Date = 09/03/15 Pct Recovery = 83% Analysis Date = 09/03/15 Pct Recovery = 83% Analysis Date = 08/29/15 Pct Recovery = 83% Analysis Date = 08/29/15 Pct Recovery = 83% Analysis Date = 08/24/15 Pct Recovery = 83% Analysis Date = 08/24/15 Pct Recovery = 83% Analysis Date = 08/19/15 Pct Recovery = 83% Analysis Date = 08/19/15 Pct Recovery = 83% Analysis Date = 08/14/15 Pct Recovery = 83% Analysis Date = 08/14/15 Pct Recovery = 83% Analysis Date = 08/09/15 Pct Recovery = 83% Analysis Date = 08/09/15 Pct Recovery = 83% Analysis Date = 08/04/15 Pct Recovery = 83% Analysis Date = 08/04/15 Pct Recovery = 83% Analysis Date = 07/31/15 Pct Recovery = 83% Analysis Date = 07/31/15 Pct Recovery = 83% Analysis Date = 07/26/15 Pct Recovery = 83% Analysis Date = 07/26/15 Pct Recovery = 83% Analysis Date = 07/21/15 Pct Recovery = 83% Analysis Date = 07/21/15 Pct Recovery = 83% Analysis Date = 07/16/15 Pct Recovery = 83% Analysis Date = 07/16/15 Pct Recovery = 83% Analysis Date = 07/11/15 Pct Recovery = 83% Analysis Date = 07/11/15 Pct Recovery = 83% Analysis Date = 07/06/15 Pct Recovery = 83% Analysis Date = 07/06/15 Pct Recovery = 83% Analysis Date = 07/01/15 Pct Recovery = 83% Analysis Date = 07/01/15 Pct Recovery = 83% Analysis Date = 06/26/15 Pct Recovery = 83% Analysis Date = 06/26/15 Pct Recovery = 83% Analysis Date = 06/21/15 Pct Recovery = 83% Analysis Date = 06/21/15 Pct Recovery = 83% Analysis Date = 06/17/15 Pct Recovery = 83% Analysis Date = 06/17/15 Pct Recovery = 83% Analysis Date = 06/12/15 Pct Recovery = 83% Analysis Date = 06/12/15 Pct Recovery = 83% Analysis Date = 06/07/15 Pct Recovery = 83% Analysis Date = 06/07/15 Pct Recovery = 83% Analysis Date = 06/02/15 Pct Recovery = 83% Analysis Date = 06/02/15 Pct Recovery = 83% Analysis Date = 05/28/15 Pct Recovery = 83% Analysis Date = 05/28/15 Pct Recovery = 83% Analysis Date = 05/23/15 Pct Recovery = 83% Analysis Date = 05/23/15 Pct Recovery = 83% Analysis Date = 05/18/15 Pct Recovery = 83% Analysis Date = 05/18/15 Pct Recovery = 83% Analysis Date = 05/13/15 Pct Recovery = 83% Analysis Date = 05/13/15 Pct Recovery = 83% Analysis Date = 05/08/15 Pct Recovery = 83% Analysis Date = 05/08/15 Pct Recovery = 83% Analysis Date = 05/04/15 Pct Recovery = 83% Analysis Date = 05/04/15 Pct Recovery = 83% Analysis Date = 04/29/15 Pct Recovery = 83% Analysis Date = 04/29/15 Pct Recovery = 83% Analysis Date = 04/24/15 Pct Recovery = 83% Analysis Date = 04/24/15 Pct Recovery = 83% Analysis Date = 04/19/15 Pct Recovery = 83% Analysis Date = 04/19/15 Pct Recovery = 83% Analysis Date = 04/14/15 Pct Recovery = 83% Analysis Date = 04/14/15 Pct Recovery = 83% Analysis Date = 04/09/15 Pct Recovery = 83% Analysis Date = 04/09/15 Pct Recovery = 83% Analysis Date = 04/04/15 Pct Recovery = 83% Analysis Date = 04/04/15 Pct Recovery = 83% Analysis Date = 03/30/15 Pct Recovery = 83% Analysis Date = 03/30/15 Pct Recovery = 83% Analysis Date = 03/25/15 Pct Recovery = 83% Analysis Date = 03/25/15 Pct Recovery = 83% Analysis Date = 03/21/15 Pct Recovery = 83% Analysis Date = 03/21/15 Pct Recovery = 83% Analysis Date = 03/16/15 Pct Recovery = 83% Analysis Date = 03/16/15 Pct Recovery = 83% Analysis Date = 03/11/15 Pct Recovery = 83% Analysis Date = 03/11/15 Pct Recovery = 83% Analysis Date = 03/06/15 Pct Recovery = 83% Analysis Date = 03/06/15 Pct Recovery = 83% Analysis Date = 03/01/15 Pct Recovery = 83% Analysis Date = 03/01/15 Pct Recovery = 83% Analysis Date = 02/24/15 Pct Recovery = 83% Analysis Date = 02/24/15 Pct Recovery = 83% Analysis Date = 02/19/15 Pct Recovery = 83% Analysis Date = 02/19/15 Pct Recovery = 83% Analysis Date = 02/14/15 Pct Recovery = 83% Analysis Date = 02/14/15 Pct Recovery = 83% Analysis Date = 02/09/15 Pct Recovery = 82% Analysis Date = 02/09/15 Pct Recovery = 82% Analysis Date = 02/05/15 Pct Recovery = 82% Analysis Date = 02/05/15 Pct Recovery = 82% Analysis Date = 01/31/15 Pct Recovery = 82% Analysis Date = 01/31/15 Pct Recovery = 82% Analysis Date = 01/26/15 Pct Recovery = 82% Analysis Date = 01/26/15 Pct Recovery = 82% Analysis Date = 01/21/15 Pct Recovery = 82% Analysis Date = 01/21/15 Pct Recovery = 82% Analysis Date = 01/16/15 Pct Recovery = 82% Analysis Date = 01/16/15 Pct Recovery = 82% Analysis Date = 01/11/15 Pct Recovery = 82% Analysis Date = 01/11/15 Pct Recovery = 82% Analysis Date = 01/06/15 Pct Recovery = 82% Analysis Date = 01/06/15 Pct Recovery = 82% Analysis Date = 01/01/15 Pct Recovery = 82% Analysis Date = 01/01/15 Pct Recovery = 82% Analysis Date = 12/27/14 Pct Recovery = 82% Analysis Date = 12/27/14 Pct Recovery = 82% Analysis Date = 12/23/14 Pct Recovery = 82% Analysis Date = 12/23/14 Pct Recovery = 82% Analysis Date = 12/18/14 Pct Recovery = 82% Analysis Date = 12/18/14 Pct Recovery = 82% Analysis Date = 12/13/14 Pct Recovery = 82% Analysis Date = 12/13/14 Pct Recovery = 82% Analysis Date = 12/08/14 Pct Recovery = 82% Analysis Date = 12/08/14 Pct Recovery = 82% Analysis Date = 12/03/14 Pct Recovery = 82% Analysis Date = 12/03/14 Pct Recovery = 82% Analysis Date = 11/28/14 Pct Recovery = 82% Analysis Date = 11/28/14 Pct Recovery = 82% Analysis Date = 11/23/14 Pct Recovery = 81% Analysis Date = 11/23/14 Pct Recovery = 81% Analysis Date = 11/18/14 Pct Recovery = 81% Analysis Date = 11/18/14 Pct Recovery = 81% Analysis Date = 11/13/14 Pct Recovery = 81% Analysis Date = 11/13/14 Pct Recovery = 81% Analysis Date = 11/09/14 Pct Recovery = 81% Analysis Date = 11/09/14 Pct Recovery = 81% Analysis Date = 11/04/14 Pct Recovery = 81% Analysis Date = 11/04/14 Pct Recovery = 81% Analysis Date = 10/30/14 Pct Recovery = 81% Analysis Date = 10/30/14 Pct Recovery = 81% Analysis Date = 10/25/14 Pct Recovery = 81% Analysis Date = 10/25/14 Pct Recovery = 81% Analysis Date = 10/20/14 Pct Recovery = 81% Analysis Date = 10/20/14 Pct Recovery = 81% Analysis Date = 10/15/14 Pct Recovery = 81% Analysis Date = 10/15/14 Pct Recovery = 81% Analysis Date = 10/10/14 Pct Recovery = 81% Analysis Date = 10/10/14 Pct Recovery = 81% Analysis Date = 10/05/14 Pct Recovery = 81% Analysis Date = 10/05/14 Pct Recovery = 81% Analysis Date = 09/30/14 Pct Recovery = 81% Analysis Date = 09/30/14 Pct Recovery = 81% Analysis Date = 09/26/14 Pct Recovery = 81% Analysis Date = 09/26/14 Pct Recovery = 81% Analysis Date = 09/21/14 Pct Recovery = 81% Analysis Date = 09/21/14 Pct Recovery = 81% Analysis Date = 09/16/14 Pct Recovery = 81% Analysis Date = 09/16/14 Pct Recovery = 81% Analysis Date = 09/11/14 Pct Recovery = 81% Analysis Date = 09/11/14 Pct Recovery = 81% Analysis Date = 09/06/14 Pct Recovery = 81% Analysis Date = 09/06/14 Pct Recovery = 81% Analysis Date = 09/01/14 Pct Recovery = 80% Analysis Date = 09/01/14 Pct Recovery = 80% Analysis Date = 08/27/14 Pct Recovery = 80% Analysis Date = 08/27/14 Pct Recovery = 80% Analysis Date = 08/22/14 Pct Recovery = 80% Analysis Date = 08/22/14 Pct Recovery = 80% Analysis Date = 08/17/14 Pct Recovery = 80% Analysis Date = 08/17/14 Pct Recovery = 80% Analysis Date = 08/13/14 Pct Recovery = 80% Analysis Date = 08/13/14 Pct Recovery = 80% Analysis Date = 08/08/14 Pct Recovery = 80% Analysis Date = 08/08/14 Pct Recovery = 80% Analysis Date = 08/03/14 Pct Recovery = 80% Analysis Date = 08/03/14 Pct Recovery = 80% Analysis Date = 07/29/14 Pct Recovery = 80% Analysis Date = 07/29/14 Pct Recovery = 80% Analysis Date = 07/24/14 Pct Recovery = 80% Analysis Date = 07/24/14 Pct Recovery = 80% Analysis Date = 07/19/14 Pct Recovery = 80% Analysis Date = 07/19/14 Pct Recovery = 80% Analysis Date = 07/14/14 Pct Recovery = 80% Analysis Date = 07/14/14 Pct Recovery = 80% Analysis Date = 07/09/14 Pct Recovery = 80% Analysis Date = 07/09/14 Pct Recovery = 80% Analysis Date = 07/04/14 Pct Recovery = 80% Analysis Date = 07/04/14 Pct Recovery = 80% Analysis Date = 06/30/14 Pct Recovery = 80% Analysis Date = 06/30/14 Pct Recovery = 80% Analysis Date = 06/25/14 Pct Recovery = 79% Analysis Date = 06/25/14 Pct Recovery = 79% Analysis Date = 06/20/14 Pct Recovery = 79% Analysis Date = 06/20/14 Pct Recovery = 79% Analysis Date = 06/15/14 Pct Recovery = 79% Analysis Date = 06/15/14 Pct Recovery = 79% Analysis Date = 06/10/14 Pct Recovery = 79% Analysis Date = 06/10/14 Pct Recovery = 79% Analysis Date = 06/05/14 Pct Recovery = 79% Analysis Date = 06/05/14 Pct Recovery = 79% Analysis Date = 05/31/14 Pct Recovery = 79% Analysis Date = 05/31/14 Pct Recovery = 79% Analysis Date = 05/26/14 Pct Recovery = 79% Analysis Date = 05/26/14 Pct Recovery = 79% Analysis Date = 05/21/14 Pct Recovery = 79% Analysis Date = 05/21/14 Pct Recovery = 79% Analysis Date = 05/17/14 Pct Recovery = 79% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
SULFAMETHOXAZOLE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 1 63% . 63% 0%
>= Reporting Level 73 80% 13% 81% 9%
Total 74 80% 13% 81% 9%

Sample Statistics
SULFAMETHOXAZOLE

Characteristic N % % Basis
Plotted 74 99% Spiked
Estimated Values 8 11% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 1 1% Spiked
Spiked 75 .  
False Negatives 0 0% 0 out of 75
Not Spiked 40 .  
False Positives 0 0% 0 out of 40

BQS OBSP Determination:
TAMOXIFEN
METHOD: 2440 , TESTIDCODE: 68015LCM56
Open Data Set

Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 26% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 25% Analysis Date = 11/04/15 SpikeMix = ERA 0406-15-07A: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 11% Analysis Date = 04/23/14 SpikeMix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.2: 20 µl Pct Recovery = 15% Analysis Date = 08/17/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 17% Analysis Date = 07/23/16 Pct Recovery = 26% Analysis Date = 07/18/16 Pct Recovery = 25% Analysis Date = 07/18/16 Pct Recovery = 25% Analysis Date = 07/14/16 Pct Recovery = 25% Analysis Date = 07/14/16 Pct Recovery = 25% Analysis Date = 07/10/16 Pct Recovery = 25% Analysis Date = 07/10/16 Pct Recovery = 25% Analysis Date = 07/06/16 Pct Recovery = 24% Analysis Date = 07/06/16 Pct Recovery = 24% Analysis Date = 07/02/16 Pct Recovery = 24% Analysis Date = 07/02/16 Pct Recovery = 24% Analysis Date = 06/28/16 Pct Recovery = 24% Analysis Date = 06/28/16 Pct Recovery = 24% Analysis Date = 06/24/16 Pct Recovery = 24% Analysis Date = 06/24/16 Pct Recovery = 24% Analysis Date = 06/20/16 Pct Recovery = 24% Analysis Date = 06/20/16 Pct Recovery = 24% Analysis Date = 06/16/16 Pct Recovery = 23% Analysis Date = 06/16/16 Pct Recovery = 23% Analysis Date = 06/11/16 Pct Recovery = 23% Analysis Date = 06/11/16 Pct Recovery = 23% Analysis Date = 06/07/16 Pct Recovery = 23% Analysis Date = 06/07/16 Pct Recovery = 23% Analysis Date = 06/03/16 Pct Recovery = 23% Analysis Date = 06/03/16 Pct Recovery = 23% Analysis Date = 05/30/16 Pct Recovery = 22% Analysis Date = 05/30/16 Pct Recovery = 22% Analysis Date = 05/26/16 Pct Recovery = 22% Analysis Date = 05/26/16 Pct Recovery = 22% Analysis Date = 05/22/16 Pct Recovery = 22% Analysis Date = 05/22/16 Pct Recovery = 22% Analysis Date = 05/18/16 Pct Recovery = 22% Analysis Date = 05/18/16 Pct Recovery = 22% Analysis Date = 05/14/16 Pct Recovery = 21% Analysis Date = 05/14/16 Pct Recovery = 21% Analysis Date = 05/10/16 Pct Recovery = 21% Analysis Date = 05/10/16 Pct Recovery = 21% Analysis Date = 05/05/16 Pct Recovery = 21% Analysis Date = 05/05/16 Pct Recovery = 21% Analysis Date = 05/01/16 Pct Recovery = 21% Analysis Date = 05/01/16 Pct Recovery = 21% Analysis Date = 04/27/16 Pct Recovery = 20% Analysis Date = 04/27/16 Pct Recovery = 20% Analysis Date = 04/23/16 Pct Recovery = 20% Analysis Date = 04/23/16 Pct Recovery = 20% Analysis Date = 04/19/16 Pct Recovery = 20% Analysis Date = 04/19/16 Pct Recovery = 20% Analysis Date = 04/15/16 Pct Recovery = 20% Analysis Date = 04/15/16 Pct Recovery = 20% Analysis Date = 04/11/16 Pct Recovery = 20% Analysis Date = 04/11/16 Pct Recovery = 20% Analysis Date = 04/07/16 Pct Recovery = 19% Analysis Date = 04/07/16 Pct Recovery = 19% Analysis Date = 04/03/16 Pct Recovery = 19% Analysis Date = 04/03/16 Pct Recovery = 19% Analysis Date = 03/29/16 Pct Recovery = 19% Analysis Date = 03/29/16 Pct Recovery = 19% Analysis Date = 03/25/16 Pct Recovery = 19% Analysis Date = 03/25/16 Pct Recovery = 19% Analysis Date = 03/21/16 Pct Recovery = 18% Analysis Date = 03/21/16 Pct Recovery = 18% Analysis Date = 03/17/16 Pct Recovery = 18% Analysis Date = 03/17/16 Pct Recovery = 18% Analysis Date = 03/13/16 Pct Recovery = 18% Analysis Date = 03/13/16 Pct Recovery = 18% Analysis Date = 03/09/16 Pct Recovery = 18% Analysis Date = 03/09/16 Pct Recovery = 18% Analysis Date = 03/05/16 Pct Recovery = 17% Analysis Date = 03/05/16 Pct Recovery = 17% Analysis Date = 03/01/16 Pct Recovery = 17% Analysis Date = 03/01/16 Pct Recovery = 17% Analysis Date = 02/26/16 Pct Recovery = 17% Analysis Date = 02/26/16 Pct Recovery = 17% Analysis Date = 02/21/16 Pct Recovery = 17% Analysis Date = 02/21/16 Pct Recovery = 17% Analysis Date = 02/17/16 Pct Recovery = 17% Analysis Date = 02/17/16 Pct Recovery = 17% Analysis Date = 02/13/16 Pct Recovery = 16% Analysis Date = 02/13/16 Pct Recovery = 16% Analysis Date = 02/09/16 Pct Recovery = 16% Analysis Date = 02/09/16 Pct Recovery = 16% Analysis Date = 02/05/16 Pct Recovery = 16% Analysis Date = 02/05/16 Pct Recovery = 16% Analysis Date = 02/01/16 Pct Recovery = 16% Analysis Date = 02/01/16 Pct Recovery = 16% Analysis Date = 01/28/16 Pct Recovery = 15% Analysis Date = 01/28/16 Pct Recovery = 15% Analysis Date = 01/24/16 Pct Recovery = 15% Analysis Date = 01/24/16 Pct Recovery = 15% Analysis Date = 01/20/16 Pct Recovery = 15% Analysis Date = 01/20/16 Pct Recovery = 15% Analysis Date = 01/15/16 Pct Recovery = 15% Analysis Date = 01/15/16 Pct Recovery = 15% Analysis Date = 01/11/16 Pct Recovery = 14% Analysis Date = 01/11/16 Pct Recovery = 14% Analysis Date = 01/07/16 Pct Recovery = 14% Analysis Date = 01/07/16 Pct Recovery = 14% Analysis Date = 01/03/16 Pct Recovery = 14% Analysis Date = 01/03/16 Pct Recovery = 14% Analysis Date = 12/30/15 Pct Recovery = 14% Analysis Date = 12/30/15 Pct Recovery = 14% Analysis Date = 12/26/15 Pct Recovery = 14% Analysis Date = 12/26/15 Pct Recovery = 14% Analysis Date = 12/22/15 Pct Recovery = 13% Analysis Date = 12/22/15 Pct Recovery = 13% Analysis Date = 12/18/15 Pct Recovery = 13% Analysis Date = 12/18/15 Pct Recovery = 13% Analysis Date = 12/14/15 Pct Recovery = 13% Analysis Date = 12/14/15 Pct Recovery = 13% Analysis Date = 12/09/15 Pct Recovery = 13% Analysis Date = 12/09/15 Pct Recovery = 13% Analysis Date = 12/05/15 Pct Recovery = 12% Analysis Date = 12/05/15 Pct Recovery = 12% Analysis Date = 12/01/15 Pct Recovery = 12% Analysis Date = 12/01/15 Pct Recovery = 12% Analysis Date = 11/27/15 Pct Recovery = 12% Analysis Date = 11/27/15 Pct Recovery = 12% Analysis Date = 11/23/15 Pct Recovery = 12% Analysis Date = 11/23/15 Pct Recovery = 12% Analysis Date = 11/19/15 Pct Recovery = 11% Analysis Date = 11/19/15 Pct Recovery = 11% Analysis Date = 11/15/15 Pct Recovery = 11% Analysis Date = 11/15/15 Pct Recovery = 11% Analysis Date = 11/11/15 Pct Recovery = 11% Analysis Date = 11/11/15 Pct Recovery = 11% Analysis Date = 11/07/15 Pct Recovery = 11% Analysis Date = 11/07/15 Pct Recovery = 11% Analysis Date = 11/02/15 Pct Recovery = 11% Analysis Date = 11/02/15 Pct Recovery = 11% Analysis Date = 10/29/15 Pct Recovery = 11% Analysis Date = 10/29/15 Pct Recovery = 11% Analysis Date = 10/25/15 Pct Recovery = 11% Analysis Date = 10/25/15 Pct Recovery = 11% Analysis Date = 10/21/15 Pct Recovery = 11% Analysis Date = 10/21/15 Pct Recovery = 11% Analysis Date = 10/17/15 Pct Recovery = 11% Analysis Date = 10/17/15 Pct Recovery = 11% Analysis Date = 10/13/15 Pct Recovery = 11% Analysis Date = 10/13/15 Pct Recovery = 11% Analysis Date = 10/09/15 Pct Recovery = 11% Analysis Date = 10/09/15 Pct Recovery = 11% Analysis Date = 10/05/15 Pct Recovery = 11% Analysis Date = 10/05/15 Pct Recovery = 11% Analysis Date = 10/01/15 Pct Recovery = 11% Analysis Date = 10/01/15 Pct Recovery = 11% Analysis Date = 09/26/15 Pct Recovery = 11% Analysis Date = 09/26/15 Pct Recovery = 11% Analysis Date = 09/22/15 Pct Recovery = 11% Analysis Date = 09/22/15 Pct Recovery = 11% Analysis Date = 09/18/15 Pct Recovery = 11% Analysis Date = 09/18/15 Pct Recovery = 11% Analysis Date = 09/14/15 Pct Recovery = 11% Analysis Date = 09/14/15 Pct Recovery = 11% Analysis Date = 09/10/15 Pct Recovery = 11% Analysis Date = 09/10/15 Pct Recovery = 11% Analysis Date = 09/06/15 Pct Recovery = 11% Analysis Date = 09/06/15 Pct Recovery = 11% Analysis Date = 09/02/15 Pct Recovery = 11% Analysis Date = 09/02/15 Pct Recovery = 11% Analysis Date = 08/29/15 Pct Recovery = 12% Analysis Date = 08/29/15 Pct Recovery = 12% Analysis Date = 08/25/15 Pct Recovery = 12% Analysis Date = 08/25/15 Pct Recovery = 12% Analysis Date = 08/20/15 Pct Recovery = 12% Analysis Date = 08/20/15 Pct Recovery = 12% Analysis Date = 08/16/15 Pct Recovery = 12% Analysis Date = 08/16/15 Pct Recovery = 12% Analysis Date = 08/12/15 Pct Recovery = 12% Analysis Date = 08/12/15 Pct Recovery = 12% Analysis Date = 08/08/15 Pct Recovery = 12% Analysis Date = 08/08/15 Pct Recovery = 12% Analysis Date = 08/04/15 Pct Recovery = 12% Analysis Date = 08/04/15 Pct Recovery = 12% Analysis Date = 07/31/15 Pct Recovery = 12% Analysis Date = 07/31/15 Pct Recovery = 12% Analysis Date = 07/27/15 Pct Recovery = 12% Analysis Date = 07/27/15 Pct Recovery = 12% Analysis Date = 07/23/15 Pct Recovery = 12% Analysis Date = 07/23/15 Pct Recovery = 12% Analysis Date = 07/19/15 Pct Recovery = 12% Analysis Date = 07/19/15 Pct Recovery = 12% Analysis Date = 07/14/15 Pct Recovery = 12% Analysis Date = 07/14/15 Pct Recovery = 12% Analysis Date = 07/10/15 Pct Recovery = 12% Analysis Date = 07/10/15 Pct Recovery = 12% Analysis Date = 07/06/15 Pct Recovery = 12% Analysis Date = 07/06/15 Pct Recovery = 12% Analysis Date = 07/02/15 Pct Recovery = 12% Analysis Date = 07/02/15 Pct Recovery = 12% Analysis Date = 06/28/15 Pct Recovery = 12% Analysis Date = 06/28/15 Pct Recovery = 12% Analysis Date = 06/24/15 Pct Recovery = 13% Analysis Date = 06/24/15 Pct Recovery = 13% Analysis Date = 06/20/15 Pct Recovery = 13% Analysis Date = 06/20/15 Pct Recovery = 13% Analysis Date = 06/16/15 Pct Recovery = 13% Analysis Date = 06/16/15 Pct Recovery = 13% Analysis Date = 06/12/15 Pct Recovery = 13% Analysis Date = 06/12/15 Pct Recovery = 13% Analysis Date = 06/08/15 Pct Recovery = 13% Analysis Date = 06/08/15 Pct Recovery = 13% Analysis Date = 06/03/15 Pct Recovery = 13% Analysis Date = 06/03/15 Pct Recovery = 13% Analysis Date = 05/30/15 Pct Recovery = 13% Analysis Date = 05/30/15 Pct Recovery = 13% Analysis Date = 05/26/15 Pct Recovery = 13% Analysis Date = 05/26/15 Pct Recovery = 13% Analysis Date = 05/22/15 Pct Recovery = 13% Analysis Date = 05/22/15 Pct Recovery = 13% Analysis Date = 05/18/15 Pct Recovery = 13% Analysis Date = 05/18/15 Pct Recovery = 13% Analysis Date = 05/14/15 Pct Recovery = 13% Analysis Date = 05/14/15 Pct Recovery = 13% Analysis Date = 05/10/15 Pct Recovery = 13% Analysis Date = 05/10/15 Pct Recovery = 13% Analysis Date = 05/06/15 Pct Recovery = 13% Analysis Date = 05/06/15 Pct Recovery = 13% Analysis Date = 05/02/15 Pct Recovery = 13% Analysis Date = 05/02/15 Pct Recovery = 13% Analysis Date = 04/27/15 Pct Recovery = 13% Analysis Date = 04/27/15 Pct Recovery = 13% Analysis Date = 04/23/15 Pct Recovery = 13% Analysis Date = 04/23/15 Pct Recovery = 13% Analysis Date = 04/19/15 Pct Recovery = 13% Analysis Date = 04/19/15 Pct Recovery = 13% Analysis Date = 04/15/15 Pct Recovery = 14% Analysis Date = 04/15/15 Pct Recovery = 14% Analysis Date = 04/11/15 Pct Recovery = 14% Analysis Date = 04/11/15 Pct Recovery = 14% Analysis Date = 04/07/15 Pct Recovery = 14% Analysis Date = 04/07/15 Pct Recovery = 14% Analysis Date = 04/03/15 Pct Recovery = 14% Analysis Date = 04/03/15 Pct Recovery = 14% Analysis Date = 03/30/15 Pct Recovery = 14% Analysis Date = 03/30/15 Pct Recovery = 14% Analysis Date = 03/26/15 Pct Recovery = 14% Analysis Date = 03/26/15 Pct Recovery = 14% Analysis Date = 03/21/15 Pct Recovery = 14% Analysis Date = 03/21/15 Pct Recovery = 14% Analysis Date = 03/17/15 Pct Recovery = 14% Analysis Date = 03/17/15 Pct Recovery = 14% Analysis Date = 03/13/15 Pct Recovery = 14% Analysis Date = 03/13/15 Pct Recovery = 14% Analysis Date = 03/09/15 Pct Recovery = 14% Analysis Date = 03/09/15 Pct Recovery = 14% Analysis Date = 03/05/15 Pct Recovery = 14% Analysis Date = 03/05/15 Pct Recovery = 14% Analysis Date = 03/01/15 Pct Recovery = 14% Analysis Date = 03/01/15 Pct Recovery = 14% Analysis Date = 02/25/15 Pct Recovery = 14% Analysis Date = 02/25/15 Pct Recovery = 14% Analysis Date = 02/21/15 Pct Recovery = 14% Analysis Date = 02/21/15 Pct Recovery = 14% Analysis Date = 02/17/15 Pct Recovery = 14% Analysis Date = 02/17/15 Pct Recovery = 14% Analysis Date = 02/12/15 Pct Recovery = 14% Analysis Date = 02/12/15 Pct Recovery = 14% Analysis Date = 02/08/15 Pct Recovery = 15% Analysis Date = 02/08/15 Pct Recovery = 15% Analysis Date = 02/04/15 Pct Recovery = 15% Analysis Date = 02/04/15 Pct Recovery = 15% Analysis Date = 01/31/15 Pct Recovery = 15% Analysis Date = 01/31/15 Pct Recovery = 15% Analysis Date = 01/27/15 Pct Recovery = 15% Analysis Date = 01/27/15 Pct Recovery = 15% Analysis Date = 01/23/15 Pct Recovery = 15% Analysis Date = 01/23/15 Pct Recovery = 15% Analysis Date = 01/19/15 Pct Recovery = 15% Analysis Date = 01/19/15 Pct Recovery = 15% Analysis Date = 01/15/15 Pct Recovery = 15% Analysis Date = 01/15/15 Pct Recovery = 15% Analysis Date = 01/11/15 Pct Recovery = 15% Analysis Date = 01/11/15 Pct Recovery = 15% Analysis Date = 01/06/15 Pct Recovery = 15% Analysis Date = 01/06/15 Pct Recovery = 15% Analysis Date = 01/02/15 Pct Recovery = 15% Analysis Date = 01/02/15 Pct Recovery = 15% Analysis Date = 12/29/14 Pct Recovery = 15% Analysis Date = 12/29/14 Pct Recovery = 15% Analysis Date = 12/25/14 Pct Recovery = 15% Analysis Date = 12/25/14 Pct Recovery = 15% Analysis Date = 12/21/14 Pct Recovery = 15% Analysis Date = 12/21/14 Pct Recovery = 15% Analysis Date = 12/17/14 Pct Recovery = 15% Analysis Date = 12/17/14 Pct Recovery = 15% Analysis Date = 12/13/14 Pct Recovery = 15% Analysis Date = 12/13/14 Pct Recovery = 15% Analysis Date = 12/09/14 Pct Recovery = 15% Analysis Date = 12/09/14 Pct Recovery = 15% Analysis Date = 12/05/14 Pct Recovery = 16% Analysis Date = 12/05/14 Pct Recovery = 16% Analysis Date = 11/30/14 Pct Recovery = 16% Analysis Date = 11/30/14 Pct Recovery = 16% Analysis Date = 11/26/14 Pct Recovery = 16% Analysis Date = 11/26/14 Pct Recovery = 16% Analysis Date = 11/22/14 Pct Recovery = 16% Analysis Date = 11/22/14 Pct Recovery = 16% Analysis Date = 11/18/14 Pct Recovery = 16% Analysis Date = 11/18/14 Pct Recovery = 16% Analysis Date = 11/14/14 Pct Recovery = 16% Analysis Date = 11/14/14 Pct Recovery = 16% Analysis Date = 11/10/14 Pct Recovery = 16% Analysis Date = 11/10/14 Pct Recovery = 16% Analysis Date = 11/06/14 Pct Recovery = 16% Analysis Date = 11/06/14 Pct Recovery = 16% Analysis Date = 11/02/14 Pct Recovery = 16% Analysis Date = 11/02/14 Pct Recovery = 16% Analysis Date = 10/29/14 Pct Recovery = 16% Analysis Date = 10/29/14 Pct Recovery = 16% Analysis Date = 10/24/14 Pct Recovery = 16% Analysis Date = 10/24/14 Pct Recovery = 16% Analysis Date = 10/20/14 Pct Recovery = 16% Analysis Date = 10/20/14 Pct Recovery = 16% Analysis Date = 10/16/14 Pct Recovery = 16% Analysis Date = 10/16/14 Pct Recovery = 16% Analysis Date = 10/12/14 Pct Recovery = 16% Analysis Date = 10/12/14 Pct Recovery = 16% Analysis Date = 10/08/14 Pct Recovery = 16% Analysis Date = 10/08/14 Pct Recovery = 16% Analysis Date = 10/04/14 Pct Recovery = 16% Analysis Date = 10/04/14 Pct Recovery = 16% Analysis Date = 09/30/14 Pct Recovery = 16% Analysis Date = 09/30/14 Pct Recovery = 16% Analysis Date = 09/26/14 Pct Recovery = 17% Analysis Date = 09/26/14 Pct Recovery = 17% Analysis Date = 09/22/14 Pct Recovery = 17% Analysis Date = 09/22/14 Pct Recovery = 17% Analysis Date = 09/17/14 Pct Recovery = 17% Analysis Date = 09/17/14 Pct Recovery = 17% Analysis Date = 09/13/14 Pct Recovery = 17% Analysis Date = 09/13/14 Pct Recovery = 17% Analysis Date = 09/09/14 Pct Recovery = 17% Analysis Date = 09/09/14 Pct Recovery = 17% Analysis Date = 09/05/14 Pct Recovery = 17% Analysis Date = 09/05/14 Pct Recovery = 17% Analysis Date = 09/01/14 Pct Recovery = 17% Analysis Date = 09/01/14 Pct Recovery = 17% Analysis Date = 08/28/14 Pct Recovery = 17% Analysis Date = 08/28/14 Pct Recovery = 17% Analysis Date = 08/24/14 Pct Recovery = 17% Analysis Date = 08/24/14 Pct Recovery = 17% Analysis Date = 08/20/14 Pct Recovery = 17% Analysis Date = 08/20/14 Pct Recovery = 17% Analysis Date = 08/16/14 Pct Recovery = 17% Analysis Date = 08/16/14 Pct Recovery = 17% Analysis Date = 08/11/14 Pct Recovery = 17% Analysis Date = 08/11/14 Pct Recovery = 17% Analysis Date = 08/07/14 Pct Recovery = 17% Analysis Date = 08/07/14 Pct Recovery = 17% Analysis Date = 08/03/14 Pct Recovery = 17% Analysis Date = 08/03/14 Pct Recovery = 17% Analysis Date = 07/30/14 Pct Recovery = 17% Analysis Date = 07/30/14 Pct Recovery = 17% Analysis Date = 07/26/14 Pct Recovery = 17% Analysis Date = 07/26/14 Pct Recovery = 17% Analysis Date = 07/22/14 Pct Recovery = 17% Analysis Date = 07/22/14 Pct Recovery = 17% Analysis Date = 07/18/14 Pct Recovery = 17% Analysis Date = 07/18/14 Pct Recovery = 17% Analysis Date = 07/14/14 Pct Recovery = 17% Analysis Date = 07/14/14 Pct Recovery = 17% Analysis Date = 07/10/14 Pct Recovery = 17% Analysis Date = 07/10/14 Pct Recovery = 17% Analysis Date = 07/05/14 Pct Recovery = 17% Analysis Date = 07/05/14 Pct Recovery = 17% Analysis Date = 07/01/14 Pct Recovery = 16% Analysis Date = 07/01/14 Pct Recovery = 16% Analysis Date = 06/27/14 Pct Recovery = 16% Analysis Date = 06/27/14 Pct Recovery = 16% Analysis Date = 06/23/14 Pct Recovery = 16% Analysis Date = 06/23/14 Pct Recovery = 16% Analysis Date = 06/19/14 Pct Recovery = 16% Analysis Date = 06/19/14 Pct Recovery = 16% Analysis Date = 06/15/14 Pct Recovery = 16% Analysis Date = 06/15/14 Pct Recovery = 16% Analysis Date = 06/11/14 Pct Recovery = 16% Analysis Date = 06/11/14 Pct Recovery = 16% Analysis Date = 06/07/14 Pct Recovery = 16% Analysis Date = 06/07/14 Pct Recovery = 16% Analysis Date = 06/03/14 Pct Recovery = 16% Analysis Date = 06/03/14 Pct Recovery = 16% Analysis Date = 05/29/14 Pct Recovery = 16% Analysis Date = 05/29/14 Pct Recovery = 16% Analysis Date = 05/25/14 Pct Recovery = 16% Analysis Date = 05/25/14 Pct Recovery = 16% Analysis Date = 05/21/14 Pct Recovery = 16% Analysis Date = 05/21/14 Pct Recovery = 16% Analysis Date = 05/17/14 Pct Recovery = 16% Analysis Date = 05/17/14 Pct Recovery = 16% Analysis Date = 05/13/14 Pct Recovery = 16% Analysis Date = 05/13/14 Pct Recovery = 16% Analysis Date = 05/09/14 Pct Recovery = 16% Analysis Date = 05/09/14 Pct Recovery = 16% Analysis Date = 05/05/14 Pct Recovery = 16% Analysis Date = 05/05/14 Pct Recovery = 16% Analysis Date = 05/01/14 Pct Recovery = 16% Analysis Date = 05/01/14 Pct Recovery = 16% Analysis Date = 04/27/14 Pct Recovery = 15% Analysis Date = 04/27/14 Pct Recovery = 15% Analysis Date = 04/23/14 Pct Recovery = 15% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
TAMOXIFEN

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 5 19% 7% 17% 7%
Total 5 19% 7% 17% 7%

Sample Statistics
TAMOXIFEN

Characteristic N % % Basis
Plotted 5 7% Spiked
Estimated Values 5 7% Spiked
Deleted Values 7 6% Spiked + Not Spiked
Spiked, Censored 5 7% Spiked
Spiked 77 .  
False Negatives 62 86% 62 out of 72
Not Spiked 38 .  
False Positives 0 0% 0 out of 36

BQS OBSP Determination:
TEMAZEPAM
METHOD: 2440 , TESTIDCODE: 67471LCM56
Open Data Set

Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 80% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 83% Analysis Date = 11/05/15 SpikeMix = ERA 0406-15-08: 80 µl & Abs 052215: 80 µl Pct Recovery = 69% Analysis Date = 11/04/15 SpikeMix = Abs 052215: 80 µl & Abs 050115: 80 µl Pct Recovery = 68% Analysis Date = 01/17/16 SpikeMix = ERA 0406-15-09: 80 µl & ERA 0406-15-07A: 80 µl Pct Recovery = 80% Analysis Date = 11/24/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 75% Analysis Date = 10/01/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 30% Analysis Date = 09/24/16 SpikeMix = Crescent EN160610015: 80 µl & Abs 061416: 80 µl Pct Recovery = 22% Analysis Date = 09/24/16 SpikeMix = Abs 061416: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 23% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 27% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 25% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 27% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 26% Analysis Date = 11/18/16 SpikeMix = ERA 04281604: 80 µl & ERA 04281603: 80 µl Pct Recovery = 78% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & ERA 04281604: 80 µl Pct Recovery = 82% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-04: 15 µl & Abs 041814: 15 µl Pct Recovery = 75% Analysis Date = 02/06/15 SpikeMix = Abs 041814: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 74% Analysis Date = 07/12/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 68% Analysis Date = 05/21/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 78% Analysis Date = 09/10/15 SpikeMix = Abs 052215: 40 µl & ERA 0406-15-07A: 40 µl Pct Recovery = 53% Analysis Date = 07/31/15 SpikeMix = Abs 051315: 40 µl & Abs 052215: 40 µl Pct Recovery = 67% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-08: 40 µl & ERA 0406-15-09: 40 µl Pct Recovery = 44% Analysis Date = 07/31/15 SpikeMix = ERA 0406-15-09: 40 µl & Abs 050115: 40 µl Pct Recovery = 66% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 17% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 20% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 17% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 17% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 21% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 22% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 116% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 117% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 80% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 91% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 82% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 79% Analysis Date = 04/10/15 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 71% Analysis Date = 11/04/14 SpikeMix = Abs 041814: 8 µl & ERA 0318-14-02: 8 µl Pct Recovery = 84% Analysis Date = 10/11/14 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 64% Analysis Date = 10/10/14 SpikeMix = Abs 041714: 30 µl & Abs 041814: 30 µl Pct Recovery = 72% Analysis Date = 10/10/14 SpikeMix = Abs 041814: 30 µl & ERA 0318-14-02: 30 µl Pct Recovery = 58% Analysis Date = 07/13/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 81% Analysis Date = 05/30/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 81% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 98% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 101% Analysis Date = 11/24/15 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 72% Analysis Date = 07/09/15 SpikeMix = Abs 050115: 20 µl & Abs 052215: 20 µl Pct Recovery = 61% Analysis Date = 06/26/15 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 53% Analysis Date = 11/24/15 SpikeMix = ERA 0406-15-09: 20 µl & Abs 050115: 20 µl Pct Recovery = 86% Analysis Date = 01/04/17 Pct Recovery = 91% Analysis Date = 12/31/16 Pct Recovery = 89% Analysis Date = 12/31/16 Pct Recovery = 89% Analysis Date = 12/26/16 Pct Recovery = 88% Analysis Date = 12/26/16 Pct Recovery = 88% Analysis Date = 12/21/16 Pct Recovery = 86% Analysis Date = 12/21/16 Pct Recovery = 86% Analysis Date = 12/16/16 Pct Recovery = 84% Analysis Date = 12/16/16 Pct Recovery = 84% Analysis Date = 12/11/16 Pct Recovery = 82% Analysis Date = 12/11/16 Pct Recovery = 82% Analysis Date = 12/07/16 Pct Recovery = 81% Analysis Date = 12/07/16 Pct Recovery = 81% Analysis Date = 12/02/16 Pct Recovery = 79% Analysis Date = 12/02/16 Pct Recovery = 79% Analysis Date = 11/27/16 Pct Recovery = 77% Analysis Date = 11/27/16 Pct Recovery = 77% Analysis Date = 11/22/16 Pct Recovery = 76% Analysis Date = 11/22/16 Pct Recovery = 76% Analysis Date = 11/17/16 Pct Recovery = 74% Analysis Date = 11/17/16 Pct Recovery = 74% Analysis Date = 11/13/16 Pct Recovery = 72% Analysis Date = 11/13/16 Pct Recovery = 72% Analysis Date = 11/08/16 Pct Recovery = 71% Analysis Date = 11/08/16 Pct Recovery = 71% Analysis Date = 11/03/16 Pct Recovery = 69% Analysis Date = 11/03/16 Pct Recovery = 69% Analysis Date = 10/29/16 Pct Recovery = 68% Analysis Date = 10/29/16 Pct Recovery = 68% Analysis Date = 10/24/16 Pct Recovery = 66% Analysis Date = 10/24/16 Pct Recovery = 66% Analysis Date = 10/20/16 Pct Recovery = 65% Analysis Date = 10/20/16 Pct Recovery = 65% Analysis Date = 10/15/16 Pct Recovery = 64% Analysis Date = 10/15/16 Pct Recovery = 64% Analysis Date = 10/10/16 Pct Recovery = 62% Analysis Date = 10/10/16 Pct Recovery = 62% Analysis Date = 10/05/16 Pct Recovery = 61% Analysis Date = 10/05/16 Pct Recovery = 61% Analysis Date = 09/30/16 Pct Recovery = 59% Analysis Date = 09/30/16 Pct Recovery = 59% Analysis Date = 09/26/16 Pct Recovery = 58% Analysis Date = 09/26/16 Pct Recovery = 58% Analysis Date = 09/21/16 Pct Recovery = 57% Analysis Date = 09/21/16 Pct Recovery = 57% Analysis Date = 09/16/16 Pct Recovery = 56% Analysis Date = 09/16/16 Pct Recovery = 56% Analysis Date = 09/11/16 Pct Recovery = 54% Analysis Date = 09/11/16 Pct Recovery = 54% Analysis Date = 09/06/16 Pct Recovery = 53% Analysis Date = 09/06/16 Pct Recovery = 53% Analysis Date = 09/02/16 Pct Recovery = 52% Analysis Date = 09/02/16 Pct Recovery = 52% Analysis Date = 08/28/16 Pct Recovery = 51% Analysis Date = 08/28/16 Pct Recovery = 51% Analysis Date = 08/23/16 Pct Recovery = 50% Analysis Date = 08/23/16 Pct Recovery = 50% Analysis Date = 08/18/16 Pct Recovery = 49% Analysis Date = 08/18/16 Pct Recovery = 49% Analysis Date = 08/13/16 Pct Recovery = 49% Analysis Date = 08/13/16 Pct Recovery = 49% Analysis Date = 08/09/16 Pct Recovery = 48% Analysis Date = 08/09/16 Pct Recovery = 48% Analysis Date = 08/04/16 Pct Recovery = 48% Analysis Date = 08/04/16 Pct Recovery = 48% Analysis Date = 07/30/16 Pct Recovery = 47% Analysis Date = 07/30/16 Pct Recovery = 47% Analysis Date = 07/25/16 Pct Recovery = 47% Analysis Date = 07/25/16 Pct Recovery = 47% Analysis Date = 07/20/16 Pct Recovery = 46% Analysis Date = 07/20/16 Pct Recovery = 46% Analysis Date = 07/16/16 Pct Recovery = 47% Analysis Date = 07/16/16 Pct Recovery = 47% Analysis Date = 07/11/16 Pct Recovery = 47% Analysis Date = 07/11/16 Pct Recovery = 47% Analysis Date = 07/06/16 Pct Recovery = 48% Analysis Date = 07/06/16 Pct Recovery = 48% Analysis Date = 07/01/16 Pct Recovery = 48% Analysis Date = 07/01/16 Pct Recovery = 48% Analysis Date = 06/26/16 Pct Recovery = 49% Analysis Date = 06/26/16 Pct Recovery = 49% Analysis Date = 06/22/16 Pct Recovery = 50% Analysis Date = 06/22/16 Pct Recovery = 50% Analysis Date = 06/17/16 Pct Recovery = 50% Analysis Date = 06/17/16 Pct Recovery = 50% Analysis Date = 06/12/16 Pct Recovery = 51% Analysis Date = 06/12/16 Pct Recovery = 51% Analysis Date = 06/07/16 Pct Recovery = 51% Analysis Date = 06/07/16 Pct Recovery = 51% Analysis Date = 06/02/16 Pct Recovery = 52% Analysis Date = 06/02/16 Pct Recovery = 52% Analysis Date = 05/29/16 Pct Recovery = 52% Analysis Date = 05/29/16 Pct Recovery = 52% Analysis Date = 05/24/16 Pct Recovery = 53% Analysis Date = 05/24/16 Pct Recovery = 53% Analysis Date = 05/19/16 Pct Recovery = 53% Analysis Date = 05/19/16 Pct Recovery = 53% Analysis Date = 05/14/16 Pct Recovery = 54% Analysis Date = 05/14/16 Pct Recovery = 54% Analysis Date = 05/09/16 Pct Recovery = 54% Analysis Date = 05/09/16 Pct Recovery = 54% Analysis Date = 05/05/16 Pct Recovery = 55% Analysis Date = 05/05/16 Pct Recovery = 55% Analysis Date = 04/30/16 Pct Recovery = 55% Analysis Date = 04/30/16 Pct Recovery = 55% Analysis Date = 04/25/16 Pct Recovery = 56% Analysis Date = 04/25/16 Pct Recovery = 56% Analysis Date = 04/20/16 Pct Recovery = 56% Analysis Date = 04/20/16 Pct Recovery = 56% Analysis Date = 04/15/16 Pct Recovery = 57% Analysis Date = 04/15/16 Pct Recovery = 57% Analysis Date = 04/11/16 Pct Recovery = 57% Analysis Date = 04/11/16 Pct Recovery = 57% Analysis Date = 04/06/16 Pct Recovery = 58% Analysis Date = 04/06/16 Pct Recovery = 58% Analysis Date = 04/01/16 Pct Recovery = 58% Analysis Date = 04/01/16 Pct Recovery = 58% Analysis Date = 03/27/16 Pct Recovery = 59% Analysis Date = 03/27/16 Pct Recovery = 59% Analysis Date = 03/22/16 Pct Recovery = 60% Analysis Date = 03/22/16 Pct Recovery = 60% Analysis Date = 03/18/16 Pct Recovery = 60% Analysis Date = 03/18/16 Pct Recovery = 60% Analysis Date = 03/13/16 Pct Recovery = 61% Analysis Date = 03/13/16 Pct Recovery = 61% Analysis Date = 03/08/16 Pct Recovery = 61% Analysis Date = 03/08/16 Pct Recovery = 61% Analysis Date = 03/03/16 Pct Recovery = 62% Analysis Date = 03/03/16 Pct Recovery = 62% Analysis Date = 02/27/16 Pct Recovery = 62% Analysis Date = 02/27/16 Pct Recovery = 62% Analysis Date = 02/23/16 Pct Recovery = 63% Analysis Date = 02/23/16 Pct Recovery = 63% Analysis Date = 02/18/16 Pct Recovery = 63% Analysis Date = 02/18/16 Pct Recovery = 63% Analysis Date = 02/13/16 Pct Recovery = 64% Analysis Date = 02/13/16 Pct Recovery = 64% Analysis Date = 02/08/16 Pct Recovery = 64% Analysis Date = 02/08/16 Pct Recovery = 64% Analysis Date = 02/03/16 Pct Recovery = 65% Analysis Date = 02/03/16 Pct Recovery = 65% Analysis Date = 01/30/16 Pct Recovery = 65% Analysis Date = 01/30/16 Pct Recovery = 65% Analysis Date = 01/25/16 Pct Recovery = 66% Analysis Date = 01/25/16 Pct Recovery = 66% Analysis Date = 01/20/16 Pct Recovery = 66% Analysis Date = 01/20/16 Pct Recovery = 66% Analysis Date = 01/15/16 Pct Recovery = 67% Analysis Date = 01/15/16 Pct Recovery = 67% Analysis Date = 01/10/16 Pct Recovery = 67% Analysis Date = 01/10/16 Pct Recovery = 67% Analysis Date = 01/06/16 Pct Recovery = 67% Analysis Date = 01/06/16 Pct Recovery = 67% Analysis Date = 01/01/16 Pct Recovery = 67% Analysis Date = 01/01/16 Pct Recovery = 67% Analysis Date = 12/27/15 Pct Recovery = 67% Analysis Date = 12/27/15 Pct Recovery = 67% Analysis Date = 12/22/15 Pct Recovery = 67% Analysis Date = 12/22/15 Pct Recovery = 67% Analysis Date = 12/17/15 Pct Recovery = 67% Analysis Date = 12/17/15 Pct Recovery = 67% Analysis Date = 12/13/15 Pct Recovery = 67% Analysis Date = 12/13/15 Pct Recovery = 67% Analysis Date = 12/08/15 Pct Recovery = 67% Analysis Date = 12/08/15 Pct Recovery = 67% Analysis Date = 12/03/15 Pct Recovery = 67% Analysis Date = 12/03/15 Pct Recovery = 67% Analysis Date = 11/28/15 Pct Recovery = 67% Analysis Date = 11/28/15 Pct Recovery = 67% Analysis Date = 11/23/15 Pct Recovery = 67% Analysis Date = 11/23/15 Pct Recovery = 67% Analysis Date = 11/19/15 Pct Recovery = 67% Analysis Date = 11/19/15 Pct Recovery = 67% Analysis Date = 11/14/15 Pct Recovery = 67% Analysis Date = 11/14/15 Pct Recovery = 67% Analysis Date = 11/09/15 Pct Recovery = 67% Analysis Date = 11/09/15 Pct Recovery = 67% Analysis Date = 11/04/15 Pct Recovery = 67% Analysis Date = 11/04/15 Pct Recovery = 67% Analysis Date = 10/30/15 Pct Recovery = 66% Analysis Date = 10/30/15 Pct Recovery = 66% Analysis Date = 10/26/15 Pct Recovery = 66% Analysis Date = 10/26/15 Pct Recovery = 66% Analysis Date = 10/21/15 Pct Recovery = 66% Analysis Date = 10/21/15 Pct Recovery = 66% Analysis Date = 10/16/15 Pct Recovery = 66% Analysis Date = 10/16/15 Pct Recovery = 66% Analysis Date = 10/11/15 Pct Recovery = 66% Analysis Date = 10/11/15 Pct Recovery = 66% Analysis Date = 10/06/15 Pct Recovery = 66% Analysis Date = 10/06/15 Pct Recovery = 66% Analysis Date = 10/02/15 Pct Recovery = 66% Analysis Date = 10/02/15 Pct Recovery = 66% Analysis Date = 09/27/15 Pct Recovery = 66% Analysis Date = 09/27/15 Pct Recovery = 66% Analysis Date = 09/22/15 Pct Recovery = 66% Analysis Date = 09/22/15 Pct Recovery = 66% Analysis Date = 09/17/15 Pct Recovery = 66% Analysis Date = 09/17/15 Pct Recovery = 66% Analysis Date = 09/12/15 Pct Recovery = 66% Analysis Date = 09/12/15 Pct Recovery = 66% Analysis Date = 09/08/15 Pct Recovery = 66% Analysis Date = 09/08/15 Pct Recovery = 66% Analysis Date = 09/03/15 Pct Recovery = 66% Analysis Date = 09/03/15 Pct Recovery = 66% Analysis Date = 08/29/15 Pct Recovery = 66% Analysis Date = 08/29/15 Pct Recovery = 66% Analysis Date = 08/24/15 Pct Recovery = 66% Analysis Date = 08/24/15 Pct Recovery = 66% Analysis Date = 08/19/15 Pct Recovery = 66% Analysis Date = 08/19/15 Pct Recovery = 66% Analysis Date = 08/15/15 Pct Recovery = 66% Analysis Date = 08/15/15 Pct Recovery = 66% Analysis Date = 08/10/15 Pct Recovery = 66% Analysis Date = 08/10/15 Pct Recovery = 66% Analysis Date = 08/05/15 Pct Recovery = 66% Analysis Date = 08/05/15 Pct Recovery = 66% Analysis Date = 07/31/15 Pct Recovery = 66% Analysis Date = 07/31/15 Pct Recovery = 66% Analysis Date = 07/26/15 Pct Recovery = 66% Analysis Date = 07/26/15 Pct Recovery = 66% Analysis Date = 07/22/15 Pct Recovery = 66% Analysis Date = 07/22/15 Pct Recovery = 66% Analysis Date = 07/17/15 Pct Recovery = 66% Analysis Date = 07/17/15 Pct Recovery = 66% Analysis Date = 07/12/15 Pct Recovery = 66% Analysis Date = 07/12/15 Pct Recovery = 66% Analysis Date = 07/07/15 Pct Recovery = 66% Analysis Date = 07/07/15 Pct Recovery = 66% Analysis Date = 07/02/15 Pct Recovery = 66% Analysis Date = 07/02/15 Pct Recovery = 66% Analysis Date = 06/28/15 Pct Recovery = 66% Analysis Date = 06/28/15 Pct Recovery = 66% Analysis Date = 06/23/15 Pct Recovery = 66% Analysis Date = 06/23/15 Pct Recovery = 66% Analysis Date = 06/18/15 Pct Recovery = 66% Analysis Date = 06/18/15 Pct Recovery = 66% Analysis Date = 06/13/15 Pct Recovery = 66% Analysis Date = 06/13/15 Pct Recovery = 66% Analysis Date = 06/08/15 Pct Recovery = 66% Analysis Date = 06/08/15 Pct Recovery = 66% Analysis Date = 06/04/15 Pct Recovery = 66% Analysis Date = 06/04/15 Pct Recovery = 66% Analysis Date = 05/30/15 Pct Recovery = 66% Analysis Date = 05/30/15 Pct Recovery = 66% Analysis Date = 05/25/15 Pct Recovery = 66% Analysis Date = 05/25/15 Pct Recovery = 66% Analysis Date = 05/20/15 Pct Recovery = 66% Analysis Date = 05/20/15 Pct Recovery = 66% Analysis Date = 05/15/15 Pct Recovery = 67% Analysis Date = 05/15/15 Pct Recovery = 67% Analysis Date = 05/11/15 Pct Recovery = 67% Analysis Date = 05/11/15 Pct Recovery = 67% Analysis Date = 05/06/15 Pct Recovery = 67% Analysis Date = 05/06/15 Pct Recovery = 67% Analysis Date = 05/01/15 Pct Recovery = 67% Analysis Date = 05/01/15 Pct Recovery = 67% Analysis Date = 04/26/15 Pct Recovery = 67% Analysis Date = 04/26/15 Pct Recovery = 67% Analysis Date = 04/21/15 Pct Recovery = 67% Analysis Date = 04/21/15 Pct Recovery = 67% Analysis Date = 04/17/15 Pct Recovery = 67% Analysis Date = 04/17/15 Pct Recovery = 67% Analysis Date = 04/12/15 Pct Recovery = 67% Analysis Date = 04/12/15 Pct Recovery = 67% Analysis Date = 04/07/15 Pct Recovery = 67% Analysis Date = 04/07/15 Pct Recovery = 67% Analysis Date = 04/02/15 Pct Recovery = 68% Analysis Date = 04/02/15 Pct Recovery = 68% Analysis Date = 03/28/15 Pct Recovery = 68% Analysis Date = 03/28/15 Pct Recovery = 68% Analysis Date = 03/24/15 Pct Recovery = 68% Analysis Date = 03/24/15 Pct Recovery = 68% Analysis Date = 03/19/15 Pct Recovery = 68% Analysis Date = 03/19/15 Pct Recovery = 68% Analysis Date = 03/14/15 Pct Recovery = 68% Analysis Date = 03/14/15 Pct Recovery = 68% Analysis Date = 03/09/15 Pct Recovery = 68% Analysis Date = 03/09/15 Pct Recovery = 68% Analysis Date = 03/04/15 Pct Recovery = 68% Analysis Date = 03/04/15 Pct Recovery = 68% Analysis Date = 02/28/15 Pct Recovery = 68% Analysis Date = 02/28/15 Pct Recovery = 68% Analysis Date = 02/23/15 Pct Recovery = 68% Analysis Date = 02/23/15 Pct Recovery = 68% Analysis Date = 02/18/15 Pct Recovery = 69% Analysis Date = 02/18/15 Pct Recovery = 69% Analysis Date = 02/13/15 Pct Recovery = 69% Analysis Date = 02/13/15 Pct Recovery = 69% Analysis Date = 02/08/15 Pct Recovery = 69% Analysis Date = 02/08/15 Pct Recovery = 69% Analysis Date = 02/04/15 Pct Recovery = 69% Analysis Date = 02/04/15 Pct Recovery = 69% Analysis Date = 01/30/15 Pct Recovery = 69% Analysis Date = 01/30/15 Pct Recovery = 69% Analysis Date = 01/25/15 Pct Recovery = 69% Analysis Date = 01/25/15 Pct Recovery = 69% Analysis Date = 01/20/15 Pct Recovery = 69% Analysis Date = 01/20/15 Pct Recovery = 69% Analysis Date = 01/15/15 Pct Recovery = 69% Analysis Date = 01/15/15 Pct Recovery = 69% Analysis Date = 01/11/15 Pct Recovery = 70% Analysis Date = 01/11/15 Pct Recovery = 70% Analysis Date = 01/06/15 Pct Recovery = 70% Analysis Date = 01/06/15 Pct Recovery = 70% Analysis Date = 01/01/15 Pct Recovery = 70% Analysis Date = 01/01/15 Pct Recovery = 70% Analysis Date = 12/27/14 Pct Recovery = 70% Analysis Date = 12/27/14 Pct Recovery = 70% Analysis Date = 12/22/14 Pct Recovery = 70% Analysis Date = 12/22/14 Pct Recovery = 70% Analysis Date = 12/18/14 Pct Recovery = 70% Analysis Date = 12/18/14 Pct Recovery = 70% Analysis Date = 12/13/14 Pct Recovery = 70% Analysis Date = 12/13/14 Pct Recovery = 70% Analysis Date = 12/08/14 Pct Recovery = 70% Analysis Date = 12/08/14 Pct Recovery = 70% Analysis Date = 12/03/14 Pct Recovery = 71% Analysis Date = 12/03/14 Pct Recovery = 71% Analysis Date = 11/28/14 Pct Recovery = 71% Analysis Date = 11/28/14 Pct Recovery = 71% Analysis Date = 11/24/14 Pct Recovery = 71% Analysis Date = 11/24/14 Pct Recovery = 71% Analysis Date = 11/19/14 Pct Recovery = 71% Analysis Date = 11/19/14 Pct Recovery = 71% Analysis Date = 11/14/14 Pct Recovery = 71% Analysis Date = 11/14/14 Pct Recovery = 71% Analysis Date = 11/09/14 Pct Recovery = 71% Analysis Date = 11/09/14 Pct Recovery = 71% Analysis Date = 11/04/14 Pct Recovery = 71% Analysis Date = 11/04/14 Pct Recovery = 71% Analysis Date = 10/31/14 Pct Recovery = 71% Analysis Date = 10/31/14 Pct Recovery = 71% Analysis Date = 10/26/14 Pct Recovery = 72% Analysis Date = 10/26/14 Pct Recovery = 72% Analysis Date = 10/21/14 Pct Recovery = 72% Analysis Date = 10/21/14 Pct Recovery = 72% Analysis Date = 10/16/14 Pct Recovery = 72% Analysis Date = 10/16/14 Pct Recovery = 72% Analysis Date = 10/11/14 Pct Recovery = 72% Analysis Date = 10/11/14 Pct Recovery = 72% Analysis Date = 10/07/14 Pct Recovery = 72% Analysis Date = 10/07/14 Pct Recovery = 72% Analysis Date = 10/02/14 Pct Recovery = 72% Analysis Date = 10/02/14 Pct Recovery = 72% Analysis Date = 09/27/14 Pct Recovery = 72% Analysis Date = 09/27/14 Pct Recovery = 72% Analysis Date = 09/22/14 Pct Recovery = 73% Analysis Date = 09/22/14 Pct Recovery = 73% Analysis Date = 09/17/14 Pct Recovery = 73% Analysis Date = 09/17/14 Pct Recovery = 73% Analysis Date = 09/13/14 Pct Recovery = 73% Analysis Date = 09/13/14 Pct Recovery = 73% Analysis Date = 09/08/14 Pct Recovery = 73% Analysis Date = 09/08/14 Pct Recovery = 73% Analysis Date = 09/03/14 Pct Recovery = 73% Analysis Date = 09/03/14 Pct Recovery = 73% Analysis Date = 08/29/14 Pct Recovery = 73% Analysis Date = 08/29/14 Pct Recovery = 73% Analysis Date = 08/24/14 Pct Recovery = 73% Analysis Date = 08/24/14 Pct Recovery = 73% Analysis Date = 08/20/14 Pct Recovery = 73% Analysis Date = 08/20/14 Pct Recovery = 73% Analysis Date = 08/15/14 Pct Recovery = 74% Analysis Date = 08/15/14 Pct Recovery = 74% Analysis Date = 08/10/14 Pct Recovery = 74% Analysis Date = 08/10/14 Pct Recovery = 74% Analysis Date = 08/05/14 Pct Recovery = 74% Analysis Date = 08/05/14 Pct Recovery = 74% Analysis Date = 07/31/14 Pct Recovery = 74% Analysis Date = 07/31/14 Pct Recovery = 74% Analysis Date = 07/27/14 Pct Recovery = 74% Analysis Date = 07/27/14 Pct Recovery = 74% Analysis Date = 07/22/14 Pct Recovery = 74% Analysis Date = 07/22/14 Pct Recovery = 74% Analysis Date = 07/17/14 Pct Recovery = 74% Analysis Date = 07/17/14 Pct Recovery = 74% Analysis Date = 07/12/14 Pct Recovery = 75% Analysis Date = 07/12/14 Pct Recovery = 75% Analysis Date = 07/07/14 Pct Recovery = 75% Analysis Date = 07/07/14 Pct Recovery = 75% Analysis Date = 07/03/14 Pct Recovery = 75% Analysis Date = 07/03/14 Pct Recovery = 75% Analysis Date = 06/28/14 Pct Recovery = 75% Analysis Date = 06/28/14 Pct Recovery = 75% Analysis Date = 06/23/14 Pct Recovery = 75% Analysis Date = 06/23/14 Pct Recovery = 75% Analysis Date = 06/18/14 Pct Recovery = 75% Analysis Date = 06/18/14 Pct Recovery = 75% Analysis Date = 06/13/14 Pct Recovery = 75% Analysis Date = 06/13/14 Pct Recovery = 75% Analysis Date = 06/09/14 Pct Recovery = 75% Analysis Date = 06/09/14 Pct Recovery = 75% Analysis Date = 06/04/14 Pct Recovery = 76% Analysis Date = 06/04/14 Pct Recovery = 76% Analysis Date = 05/30/14 Pct Recovery = 76% Analysis Date = 05/30/14 Pct Recovery = 76% Analysis Date = 05/25/14 Pct Recovery = 76% Analysis Date = 05/25/14 Pct Recovery = 76% Analysis Date = 05/21/14 Pct Recovery = 76% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
TEMAZEPAM

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 48 62% 28% 70% 39%
Total 48 62% 28% 70% 39%

Sample Statistics
TEMAZEPAM

Characteristic N % % Basis
Plotted 48 77% Spiked
Estimated Values 4 6% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 10 16% Spiked
Spiked 62 .  
False Negatives 4 6% 4 out of 62
Not Spiked 53 .  
False Positives 0 0% 0 out of 53

BQS OBSP Determination:
THEOPHYLLINE
METHOD: 2440 , TESTIDCODE: 67494LCM56
Open Data Set

Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 58% Analysis Date = 11/24/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 89% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 80 µl & Abs 051315: 80 µl Pct Recovery = 91% Analysis Date = 10/01/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 75% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 80 µl & ERA 0406-15-08: 80 µl Pct Recovery = 54% Analysis Date = 11/05/15 SpikeMix = ERA 0406-15-08: 80 µl & Abs 052215: 80 µl Pct Recovery = 61% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 99% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 102% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 96% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 97% Analysis Date = 11/18/16 SpikeMix = ERA 04281604: 80 µl & ERA 04281603: 80 µl Pct Recovery = 50% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & ERA 04281604: 80 µl Pct Recovery = 53% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 42% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 45% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-04: 15 µl & Abs 041814: 15 µl Pct Recovery = 90% Analysis Date = 02/06/15 SpikeMix = Abs 041814: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 90% Analysis Date = 07/12/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 70% Analysis Date = 05/21/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 82% Analysis Date = 05/07/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 118% Analysis Date = 04/29/15 SpikeMix = ERA 0319-14-05: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 123% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 94% Analysis Date = 01/16/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 91% Analysis Date = 12/07/14 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 92% Analysis Date = 12/06/14 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 83% Analysis Date = 08/28/14 SpikeMix = ERA 0319-14-04: 60 µl & ERA 0319-14-05: 60 µl Pct Recovery = 80% Analysis Date = 07/26/14 SpikeMix = ERA 0319-14-05: 60 µl & ERA 0318-14-02: 60 µl Pct Recovery = 90% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 86% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 75% Analysis Date = 07/31/15 SpikeMix = Abs 051315: 40 µl & Abs 052215: 40 µl Pct Recovery = 80% Analysis Date = 07/30/15 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 87% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-08: 40 µl & Abs 052215: 40 µl Pct Recovery = 50% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 115% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 124% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 92% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 89% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 71% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 87% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 62% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 60% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 43% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 45% Analysis Date = 11/04/14 SpikeMix = Abs 041814: 8 µl & ERA 0318-14-02: 8 µl Pct Recovery = 76% Analysis Date = 10/11/14 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 85% Analysis Date = 11/04/14 SpikeMix = Abs 041714: 8 µl & ERA 0319-14-05: 8 µl Pct Recovery = 81% Analysis Date = 10/24/14 SpikeMix = ERA 0319-14-05: 8 µl & Abs 041614: 8 µl Pct Recovery = 94% Analysis Date = 10/10/14 SpikeMix = Abs 041714: 30 µl & Abs 041814: 30 µl Pct Recovery = 82% Analysis Date = 07/13/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 81% Analysis Date = 08/30/14 SpikeMix = ERA 0318-14-02: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 83% Analysis Date = 08/16/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 55% Analysis Date = 07/13/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 74% Analysis Date = 02/23/16 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 70% Analysis Date = 06/26/15 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 117% Analysis Date = 06/09/15 SpikeMix = Abs 051315: 20 µl & Abs 050115: 20 µl Pct Recovery = 86% Analysis Date = 01/18/17 Pct Recovery = 70% Analysis Date = 01/14/17 Pct Recovery = 70% Analysis Date = 01/14/17 Pct Recovery = 70% Analysis Date = 01/09/17 Pct Recovery = 70% Analysis Date = 01/09/17 Pct Recovery = 70% Analysis Date = 01/04/17 Pct Recovery = 71% Analysis Date = 01/04/17 Pct Recovery = 71% Analysis Date = 12/30/16 Pct Recovery = 71% Analysis Date = 12/30/16 Pct Recovery = 71% Analysis Date = 12/25/16 Pct Recovery = 71% Analysis Date = 12/25/16 Pct Recovery = 71% Analysis Date = 12/20/16 Pct Recovery = 71% Analysis Date = 12/20/16 Pct Recovery = 71% Analysis Date = 12/15/16 Pct Recovery = 71% Analysis Date = 12/15/16 Pct Recovery = 71% Analysis Date = 12/11/16 Pct Recovery = 71% Analysis Date = 12/11/16 Pct Recovery = 71% Analysis Date = 12/06/16 Pct Recovery = 72% Analysis Date = 12/06/16 Pct Recovery = 72% Analysis Date = 12/01/16 Pct Recovery = 72% Analysis Date = 12/01/16 Pct Recovery = 72% Analysis Date = 11/26/16 Pct Recovery = 72% Analysis Date = 11/26/16 Pct Recovery = 72% Analysis Date = 11/21/16 Pct Recovery = 72% Analysis Date = 11/21/16 Pct Recovery = 72% Analysis Date = 11/16/16 Pct Recovery = 72% Analysis Date = 11/16/16 Pct Recovery = 72% Analysis Date = 11/11/16 Pct Recovery = 72% Analysis Date = 11/11/16 Pct Recovery = 72% Analysis Date = 11/06/16 Pct Recovery = 72% Analysis Date = 11/06/16 Pct Recovery = 72% Analysis Date = 11/02/16 Pct Recovery = 73% Analysis Date = 11/02/16 Pct Recovery = 73% Analysis Date = 10/28/16 Pct Recovery = 73% Analysis Date = 10/28/16 Pct Recovery = 73% Analysis Date = 10/23/16 Pct Recovery = 73% Analysis Date = 10/23/16 Pct Recovery = 73% Analysis Date = 10/18/16 Pct Recovery = 73% Analysis Date = 10/18/16 Pct Recovery = 73% Analysis Date = 10/13/16 Pct Recovery = 73% Analysis Date = 10/13/16 Pct Recovery = 73% Analysis Date = 10/08/16 Pct Recovery = 73% Analysis Date = 10/08/16 Pct Recovery = 73% Analysis Date = 10/03/16 Pct Recovery = 73% Analysis Date = 10/03/16 Pct Recovery = 73% Analysis Date = 09/28/16 Pct Recovery = 73% Analysis Date = 09/28/16 Pct Recovery = 73% Analysis Date = 09/24/16 Pct Recovery = 74% Analysis Date = 09/24/16 Pct Recovery = 74% Analysis Date = 09/19/16 Pct Recovery = 74% Analysis Date = 09/19/16 Pct Recovery = 74% Analysis Date = 09/14/16 Pct Recovery = 74% Analysis Date = 09/14/16 Pct Recovery = 74% Analysis Date = 09/09/16 Pct Recovery = 74% Analysis Date = 09/09/16 Pct Recovery = 74% Analysis Date = 09/04/16 Pct Recovery = 74% Analysis Date = 09/04/16 Pct Recovery = 74% Analysis Date = 08/30/16 Pct Recovery = 74% Analysis Date = 08/30/16 Pct Recovery = 74% Analysis Date = 08/25/16 Pct Recovery = 74% Analysis Date = 08/25/16 Pct Recovery = 74% Analysis Date = 08/21/16 Pct Recovery = 74% Analysis Date = 08/21/16 Pct Recovery = 74% Analysis Date = 08/16/16 Pct Recovery = 74% Analysis Date = 08/16/16 Pct Recovery = 74% Analysis Date = 08/11/16 Pct Recovery = 74% Analysis Date = 08/11/16 Pct Recovery = 74% Analysis Date = 08/06/16 Pct Recovery = 74% Analysis Date = 08/06/16 Pct Recovery = 74% Analysis Date = 08/01/16 Pct Recovery = 74% Analysis Date = 08/01/16 Pct Recovery = 74% Analysis Date = 07/27/16 Pct Recovery = 74% Analysis Date = 07/27/16 Pct Recovery = 74% Analysis Date = 07/22/16 Pct Recovery = 74% Analysis Date = 07/22/16 Pct Recovery = 74% Analysis Date = 07/17/16 Pct Recovery = 74% Analysis Date = 07/17/16 Pct Recovery = 74% Analysis Date = 07/13/16 Pct Recovery = 74% Analysis Date = 07/13/16 Pct Recovery = 74% Analysis Date = 07/08/16 Pct Recovery = 74% Analysis Date = 07/08/16 Pct Recovery = 74% Analysis Date = 07/03/16 Pct Recovery = 75% Analysis Date = 07/03/16 Pct Recovery = 75% Analysis Date = 06/28/16 Pct Recovery = 75% Analysis Date = 06/28/16 Pct Recovery = 75% Analysis Date = 06/23/16 Pct Recovery = 75% Analysis Date = 06/23/16 Pct Recovery = 75% Analysis Date = 06/18/16 Pct Recovery = 75% Analysis Date = 06/18/16 Pct Recovery = 75% Analysis Date = 06/13/16 Pct Recovery = 75% Analysis Date = 06/13/16 Pct Recovery = 75% Analysis Date = 06/08/16 Pct Recovery = 75% Analysis Date = 06/08/16 Pct Recovery = 75% Analysis Date = 06/04/16 Pct Recovery = 75% Analysis Date = 06/04/16 Pct Recovery = 75% Analysis Date = 05/30/16 Pct Recovery = 75% Analysis Date = 05/30/16 Pct Recovery = 75% Analysis Date = 05/25/16 Pct Recovery = 75% Analysis Date = 05/25/16 Pct Recovery = 75% Analysis Date = 05/20/16 Pct Recovery = 75% Analysis Date = 05/20/16 Pct Recovery = 75% Analysis Date = 05/15/16 Pct Recovery = 75% Analysis Date = 05/15/16 Pct Recovery = 75% Analysis Date = 05/10/16 Pct Recovery = 75% Analysis Date = 05/10/16 Pct Recovery = 75% Analysis Date = 05/05/16 Pct Recovery = 75% Analysis Date = 05/05/16 Pct Recovery = 75% Analysis Date = 05/01/16 Pct Recovery = 75% Analysis Date = 05/01/16 Pct Recovery = 75% Analysis Date = 04/26/16 Pct Recovery = 75% Analysis Date = 04/26/16 Pct Recovery = 75% Analysis Date = 04/21/16 Pct Recovery = 75% Analysis Date = 04/21/16 Pct Recovery = 75% Analysis Date = 04/16/16 Pct Recovery = 75% Analysis Date = 04/16/16 Pct Recovery = 75% Analysis Date = 04/11/16 Pct Recovery = 75% Analysis Date = 04/11/16 Pct Recovery = 75% Analysis Date = 04/06/16 Pct Recovery = 75% Analysis Date = 04/06/16 Pct Recovery = 75% Analysis Date = 04/01/16 Pct Recovery = 75% Analysis Date = 04/01/16 Pct Recovery = 75% Analysis Date = 03/27/16 Pct Recovery = 75% Analysis Date = 03/27/16 Pct Recovery = 75% Analysis Date = 03/23/16 Pct Recovery = 75% Analysis Date = 03/23/16 Pct Recovery = 75% Analysis Date = 03/18/16 Pct Recovery = 75% Analysis Date = 03/18/16 Pct Recovery = 75% Analysis Date = 03/13/16 Pct Recovery = 75% Analysis Date = 03/13/16 Pct Recovery = 75% Analysis Date = 03/08/16 Pct Recovery = 75% Analysis Date = 03/08/16 Pct Recovery = 75% Analysis Date = 03/03/16 Pct Recovery = 75% Analysis Date = 03/03/16 Pct Recovery = 75% Analysis Date = 02/27/16 Pct Recovery = 75% Analysis Date = 02/27/16 Pct Recovery = 75% Analysis Date = 02/22/16 Pct Recovery = 75% Analysis Date = 02/22/16 Pct Recovery = 75% Analysis Date = 02/17/16 Pct Recovery = 75% Analysis Date = 02/17/16 Pct Recovery = 75% Analysis Date = 02/13/16 Pct Recovery = 76% Analysis Date = 02/13/16 Pct Recovery = 76% Analysis Date = 02/08/16 Pct Recovery = 76% Analysis Date = 02/08/16 Pct Recovery = 76% Analysis Date = 02/03/16 Pct Recovery = 76% Analysis Date = 02/03/16 Pct Recovery = 76% Analysis Date = 01/29/16 Pct Recovery = 77% Analysis Date = 01/29/16 Pct Recovery = 77% Analysis Date = 01/24/16 Pct Recovery = 77% Analysis Date = 01/24/16 Pct Recovery = 77% Analysis Date = 01/19/16 Pct Recovery = 77% Analysis Date = 01/19/16 Pct Recovery = 77% Analysis Date = 01/14/16 Pct Recovery = 77% Analysis Date = 01/14/16 Pct Recovery = 77% Analysis Date = 01/10/16 Pct Recovery = 78% Analysis Date = 01/10/16 Pct Recovery = 78% Analysis Date = 01/05/16 Pct Recovery = 78% Analysis Date = 01/05/16 Pct Recovery = 78% Analysis Date = 12/31/15 Pct Recovery = 78% Analysis Date = 12/31/15 Pct Recovery = 78% Analysis Date = 12/26/15 Pct Recovery = 79% Analysis Date = 12/26/15 Pct Recovery = 79% Analysis Date = 12/21/15 Pct Recovery = 79% Analysis Date = 12/21/15 Pct Recovery = 79% Analysis Date = 12/16/15 Pct Recovery = 79% Analysis Date = 12/16/15 Pct Recovery = 79% Analysis Date = 12/11/15 Pct Recovery = 79% Analysis Date = 12/11/15 Pct Recovery = 79% Analysis Date = 12/06/15 Pct Recovery = 80% Analysis Date = 12/06/15 Pct Recovery = 80% Analysis Date = 12/02/15 Pct Recovery = 80% Analysis Date = 12/02/15 Pct Recovery = 80% Analysis Date = 11/27/15 Pct Recovery = 80% Analysis Date = 11/27/15 Pct Recovery = 80% Analysis Date = 11/22/15 Pct Recovery = 81% Analysis Date = 11/22/15 Pct Recovery = 81% Analysis Date = 11/17/15 Pct Recovery = 81% Analysis Date = 11/17/15 Pct Recovery = 81% Analysis Date = 11/12/15 Pct Recovery = 81% Analysis Date = 11/12/15 Pct Recovery = 81% Analysis Date = 11/07/15 Pct Recovery = 81% Analysis Date = 11/07/15 Pct Recovery = 81% Analysis Date = 11/02/15 Pct Recovery = 82% Analysis Date = 11/02/15 Pct Recovery = 82% Analysis Date = 10/28/15 Pct Recovery = 82% Analysis Date = 10/28/15 Pct Recovery = 82% Analysis Date = 10/24/15 Pct Recovery = 82% Analysis Date = 10/24/15 Pct Recovery = 82% Analysis Date = 10/19/15 Pct Recovery = 83% Analysis Date = 10/19/15 Pct Recovery = 83% Analysis Date = 10/14/15 Pct Recovery = 83% Analysis Date = 10/14/15 Pct Recovery = 83% Analysis Date = 10/09/15 Pct Recovery = 83% Analysis Date = 10/09/15 Pct Recovery = 83% Analysis Date = 10/04/15 Pct Recovery = 83% Analysis Date = 10/04/15 Pct Recovery = 83% Analysis Date = 09/29/15 Pct Recovery = 84% Analysis Date = 09/29/15 Pct Recovery = 84% Analysis Date = 09/24/15 Pct Recovery = 84% Analysis Date = 09/24/15 Pct Recovery = 84% Analysis Date = 09/19/15 Pct Recovery = 84% Analysis Date = 09/19/15 Pct Recovery = 84% Analysis Date = 09/15/15 Pct Recovery = 85% Analysis Date = 09/15/15 Pct Recovery = 85% Analysis Date = 09/10/15 Pct Recovery = 85% Analysis Date = 09/10/15 Pct Recovery = 85% Analysis Date = 09/05/15 Pct Recovery = 85% Analysis Date = 09/05/15 Pct Recovery = 85% Analysis Date = 08/31/15 Pct Recovery = 85% Analysis Date = 08/31/15 Pct Recovery = 85% Analysis Date = 08/26/15 Pct Recovery = 86% Analysis Date = 08/26/15 Pct Recovery = 86% Analysis Date = 08/21/15 Pct Recovery = 86% Analysis Date = 08/21/15 Pct Recovery = 86% Analysis Date = 08/16/15 Pct Recovery = 86% Analysis Date = 08/16/15 Pct Recovery = 86% Analysis Date = 08/12/15 Pct Recovery = 86% Analysis Date = 08/12/15 Pct Recovery = 86% Analysis Date = 08/07/15 Pct Recovery = 87% Analysis Date = 08/07/15 Pct Recovery = 87% Analysis Date = 08/02/15 Pct Recovery = 87% Analysis Date = 08/02/15 Pct Recovery = 87% Analysis Date = 07/28/15 Pct Recovery = 87% Analysis Date = 07/28/15 Pct Recovery = 87% Analysis Date = 07/23/15 Pct Recovery = 88% Analysis Date = 07/23/15 Pct Recovery = 88% Analysis Date = 07/18/15 Pct Recovery = 88% Analysis Date = 07/18/15 Pct Recovery = 88% Analysis Date = 07/13/15 Pct Recovery = 88% Analysis Date = 07/13/15 Pct Recovery = 88% Analysis Date = 07/08/15 Pct Recovery = 88% Analysis Date = 07/08/15 Pct Recovery = 88% Analysis Date = 07/04/15 Pct Recovery = 89% Analysis Date = 07/04/15 Pct Recovery = 89% Analysis Date = 06/29/15 Pct Recovery = 89% Analysis Date = 06/29/15 Pct Recovery = 89% Analysis Date = 06/24/15 Pct Recovery = 89% Analysis Date = 06/24/15 Pct Recovery = 89% Analysis Date = 06/19/15 Pct Recovery = 90% Analysis Date = 06/19/15 Pct Recovery = 90% Analysis Date = 06/14/15 Pct Recovery = 90% Analysis Date = 06/14/15 Pct Recovery = 90% Analysis Date = 06/09/15 Pct Recovery = 90% Analysis Date = 06/09/15 Pct Recovery = 90% Analysis Date = 06/04/15 Pct Recovery = 90% Analysis Date = 06/04/15 Pct Recovery = 90% Analysis Date = 05/30/15 Pct Recovery = 91% Analysis Date = 05/30/15 Pct Recovery = 91% Analysis Date = 05/26/15 Pct Recovery = 91% Analysis Date = 05/26/15 Pct Recovery = 91% Analysis Date = 05/21/15 Pct Recovery = 91% Analysis Date = 05/21/15 Pct Recovery = 91% Analysis Date = 05/16/15 Pct Recovery = 92% Analysis Date = 05/16/15 Pct Recovery = 92% Analysis Date = 05/11/15 Pct Recovery = 92% Analysis Date = 05/11/15 Pct Recovery = 92% Analysis Date = 05/06/15 Pct Recovery = 92% Analysis Date = 05/06/15 Pct Recovery = 92% Analysis Date = 05/01/15 Pct Recovery = 92% Analysis Date = 05/01/15 Pct Recovery = 92% Analysis Date = 04/26/15 Pct Recovery = 92% Analysis Date = 04/26/15 Pct Recovery = 92% Analysis Date = 04/22/15 Pct Recovery = 92% Analysis Date = 04/22/15 Pct Recovery = 92% Analysis Date = 04/17/15 Pct Recovery = 92% Analysis Date = 04/17/15 Pct Recovery = 92% Analysis Date = 04/12/15 Pct Recovery = 91% Analysis Date = 04/12/15 Pct Recovery = 91% Analysis Date = 04/07/15 Pct Recovery = 91% Analysis Date = 04/07/15 Pct Recovery = 91% Analysis Date = 04/02/15 Pct Recovery = 91% Analysis Date = 04/02/15 Pct Recovery = 91% Analysis Date = 03/28/15 Pct Recovery = 91% Analysis Date = 03/28/15 Pct Recovery = 91% Analysis Date = 03/23/15 Pct Recovery = 91% Analysis Date = 03/23/15 Pct Recovery = 91% Analysis Date = 03/18/15 Pct Recovery = 91% Analysis Date = 03/18/15 Pct Recovery = 91% Analysis Date = 03/14/15 Pct Recovery = 91% Analysis Date = 03/14/15 Pct Recovery = 91% Analysis Date = 03/09/15 Pct Recovery = 90% Analysis Date = 03/09/15 Pct Recovery = 90% Analysis Date = 03/04/15 Pct Recovery = 90% Analysis Date = 03/04/15 Pct Recovery = 90% Analysis Date = 02/27/15 Pct Recovery = 90% Analysis Date = 02/27/15 Pct Recovery = 90% Analysis Date = 02/22/15 Pct Recovery = 90% Analysis Date = 02/22/15 Pct Recovery = 90% Analysis Date = 02/17/15 Pct Recovery = 90% Analysis Date = 02/17/15 Pct Recovery = 90% Analysis Date = 02/12/15 Pct Recovery = 89% Analysis Date = 02/12/15 Pct Recovery = 89% Analysis Date = 02/07/15 Pct Recovery = 89% Analysis Date = 02/07/15 Pct Recovery = 89% Analysis Date = 02/03/15 Pct Recovery = 89% Analysis Date = 02/03/15 Pct Recovery = 89% Analysis Date = 01/29/15 Pct Recovery = 89% Analysis Date = 01/29/15 Pct Recovery = 89% Analysis Date = 01/24/15 Pct Recovery = 88% Analysis Date = 01/24/15 Pct Recovery = 88% Analysis Date = 01/19/15 Pct Recovery = 88% Analysis Date = 01/19/15 Pct Recovery = 88% Analysis Date = 01/14/15 Pct Recovery = 88% Analysis Date = 01/14/15 Pct Recovery = 88% Analysis Date = 01/09/15 Pct Recovery = 88% Analysis Date = 01/09/15 Pct Recovery = 88% Analysis Date = 01/04/15 Pct Recovery = 88% Analysis Date = 01/04/15 Pct Recovery = 88% Analysis Date = 12/31/14 Pct Recovery = 87% Analysis Date = 12/31/14 Pct Recovery = 87% Analysis Date = 12/26/14 Pct Recovery = 87% Analysis Date = 12/26/14 Pct Recovery = 87% Analysis Date = 12/21/14 Pct Recovery = 87% Analysis Date = 12/21/14 Pct Recovery = 87% Analysis Date = 12/16/14 Pct Recovery = 87% Analysis Date = 12/16/14 Pct Recovery = 87% Analysis Date = 12/11/14 Pct Recovery = 87% Analysis Date = 12/11/14 Pct Recovery = 87% Analysis Date = 12/06/14 Pct Recovery = 86% Analysis Date = 12/06/14 Pct Recovery = 86% Analysis Date = 12/01/14 Pct Recovery = 86% Analysis Date = 12/01/14 Pct Recovery = 86% Analysis Date = 11/26/14 Pct Recovery = 86% Analysis Date = 11/26/14 Pct Recovery = 86% Analysis Date = 11/22/14 Pct Recovery = 86% Analysis Date = 11/22/14 Pct Recovery = 86% Analysis Date = 11/17/14 Pct Recovery = 85% Analysis Date = 11/17/14 Pct Recovery = 85% Analysis Date = 11/12/14 Pct Recovery = 85% Analysis Date = 11/12/14 Pct Recovery = 85% Analysis Date = 11/07/14 Pct Recovery = 85% Analysis Date = 11/07/14 Pct Recovery = 85% Analysis Date = 11/02/14 Pct Recovery = 85% Analysis Date = 11/02/14 Pct Recovery = 85% Analysis Date = 10/28/14 Pct Recovery = 84% Analysis Date = 10/28/14 Pct Recovery = 84% Analysis Date = 10/23/14 Pct Recovery = 84% Analysis Date = 10/23/14 Pct Recovery = 84% Analysis Date = 10/18/14 Pct Recovery = 84% Analysis Date = 10/18/14 Pct Recovery = 84% Analysis Date = 10/14/14 Pct Recovery = 84% Analysis Date = 10/14/14 Pct Recovery = 84% Analysis Date = 10/09/14 Pct Recovery = 83% Analysis Date = 10/09/14 Pct Recovery = 83% Analysis Date = 10/04/14 Pct Recovery = 83% Analysis Date = 10/04/14 Pct Recovery = 83% Analysis Date = 09/29/14 Pct Recovery = 83% Analysis Date = 09/29/14 Pct Recovery = 83% Analysis Date = 09/24/14 Pct Recovery = 82% Analysis Date = 09/24/14 Pct Recovery = 82% Analysis Date = 09/19/14 Pct Recovery = 82% Analysis Date = 09/19/14 Pct Recovery = 82% Analysis Date = 09/14/14 Pct Recovery = 82% Analysis Date = 09/14/14 Pct Recovery = 82% Analysis Date = 09/10/14 Pct Recovery = 82% Analysis Date = 09/10/14 Pct Recovery = 82% Analysis Date = 09/05/14 Pct Recovery = 81% Analysis Date = 09/05/14 Pct Recovery = 81% Analysis Date = 08/31/14 Pct Recovery = 81% Analysis Date = 08/31/14 Pct Recovery = 81% Analysis Date = 08/26/14 Pct Recovery = 81% Analysis Date = 08/26/14 Pct Recovery = 81% Analysis Date = 08/21/14 Pct Recovery = 81% Analysis Date = 08/21/14 Pct Recovery = 81% Analysis Date = 08/16/14 Pct Recovery = 80% Analysis Date = 08/16/14 Pct Recovery = 80% Analysis Date = 08/11/14 Pct Recovery = 80% Analysis Date = 08/11/14 Pct Recovery = 80% Analysis Date = 08/06/14 Pct Recovery = 80% Analysis Date = 08/06/14 Pct Recovery = 80% Analysis Date = 08/02/14 Pct Recovery = 79% Analysis Date = 08/02/14 Pct Recovery = 79% Analysis Date = 07/28/14 Pct Recovery = 79% Analysis Date = 07/28/14 Pct Recovery = 79% Analysis Date = 07/23/14 Pct Recovery = 79% Analysis Date = 07/23/14 Pct Recovery = 79% Analysis Date = 07/18/14 Pct Recovery = 78% Analysis Date = 07/18/14 Pct Recovery = 78% Analysis Date = 07/13/14 Pct Recovery = 78% Analysis Date = 07/13/14 Pct Recovery = 78% Analysis Date = 07/08/14 Pct Recovery = 78% Analysis Date = 07/08/14 Pct Recovery = 78% Analysis Date = 07/03/14 Pct Recovery = 78% Analysis Date = 07/03/14 Pct Recovery = 78% Analysis Date = 06/28/14 Pct Recovery = 77% Analysis Date = 06/28/14 Pct Recovery = 77% Analysis Date = 06/24/14 Pct Recovery = 77% Analysis Date = 06/24/14 Pct Recovery = 77% Analysis Date = 06/19/14 Pct Recovery = 77% Analysis Date = 06/19/14 Pct Recovery = 77% Analysis Date = 06/14/14 Pct Recovery = 76% Analysis Date = 06/14/14 Pct Recovery = 76% Analysis Date = 06/09/14 Pct Recovery = 76% Analysis Date = 06/09/14 Pct Recovery = 76% Analysis Date = 06/04/14 Pct Recovery = 76% Analysis Date = 06/04/14 Pct Recovery = 76% Analysis Date = 05/30/14 Pct Recovery = 75% Analysis Date = 05/30/14 Pct Recovery = 75% Analysis Date = 05/25/14 Pct Recovery = 75% Analysis Date = 05/25/14 Pct Recovery = 75% Analysis Date = 05/21/14 Pct Recovery = 75% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
THEOPHYLLINE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 53 80% 20% 83% 16%
Total 53 80% 20% 83% 16%

Sample Statistics
THEOPHYLLINE

Characteristic N % % Basis
Plotted 53 71% Spiked
Estimated Values 12 16% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 11 15% Spiked
Spiked 75 .  
False Negatives 11 15% 11 out of 75
Not Spiked 40 .  
False Positives 1 3% 1 out of 40

BQS OBSP Determination:
THIABENDAZOLE
METHOD: 2440 , TESTIDCODE: 67455LCM56
Open Data Set

Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 80% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 83% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 82% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 78% Analysis Date = 01/17/16 SpikeMix = ERA 0406-15-09: 80 µl & ERA 0406-15-07A: 80 µl Pct Recovery = 71% Analysis Date = 11/24/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 76% Analysis Date = 10/01/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 42% Analysis Date = 11/05/15 SpikeMix = ERA 0406-15-08: 80 µl & Abs 052215: 80 µl Pct Recovery = 74% Analysis Date = 11/04/15 SpikeMix = Abs 052215: 80 µl & Abs 050115: 80 µl Pct Recovery = 83% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 76% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 73% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 72% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 74% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 79% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 73% Analysis Date = 09/24/16 SpikeMix = Crescent EN160610015: 80 µl & Abs 061416: 80 µl Pct Recovery = 64% Analysis Date = 09/24/16 SpikeMix = Abs 061416: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 50% Analysis Date = 04/29/15 SpikeMix = ERA 0319-14-05: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 95% Analysis Date = 02/06/15 SpikeMix = Abs 041814: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 71% Analysis Date = 12/06/14 SpikeMix = ERA 0318-14-02: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 46% Analysis Date = 10/11/14 SpikeMix = ERA 0318-14-02: 60 µl & ERA 0319-14-04: 60 µl Pct Recovery = 40% Analysis Date = 08/21/14 SpikeMix = ERA 0318-14-02: 60 µl & Abs 041714: 60 µl Pct Recovery = 70% Analysis Date = 07/26/14 SpikeMix = ERA 0319-14-05: 60 µl & ERA 0318-14-02: 60 µl Pct Recovery = 76% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 79% Analysis Date = 12/07/14 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 64% Analysis Date = 10/25/14 SpikeMix = Abs 041614: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 60% Analysis Date = 06/22/14 SpikeMix = Abs 041814: 60 µl & Abs 041614: 60 µl Pct Recovery = 120% Analysis Date = 06/11/14 SpikeMix = Abs 041614: 60 µl & Abs 041714: 60 µl Pct Recovery = 78% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-08: 40 µl & ERA 0406-15-09: 40 µl Pct Recovery = 83% Analysis Date = 07/31/15 SpikeMix = ERA 0406-15-09: 40 µl & Abs 050115: 40 µl Pct Recovery = 88% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-08: 40 µl & Abs 052215: 40 µl Pct Recovery = 80% Analysis Date = 02/23/16 SpikeMix = Abs 052215: 40 µl & Abs 050115: 40 µl Pct Recovery = 108% Analysis Date = 07/31/15 SpikeMix = Abs 051315: 40 µl & Abs 052215: 40 µl Pct Recovery = 48% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 76% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 74% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 72% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 69% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 60% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 63% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 62% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 75% Analysis Date = 10/10/14 SpikeMix = Abs 041814: 30 µl & ERA 0318-14-02: 30 µl Pct Recovery = 16% Analysis Date = 08/30/14 SpikeMix = ERA 0318-14-02: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 71% Analysis Date = 07/20/14 SpikeMix = ERA 0318-14-02: 30 µl & Abs 041714: 30 µl Pct Recovery = 97% Analysis Date = 04/30/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 117% Analysis Date = 09/12/14 SpikeMix = Abs 041614: 30 µl & ERA 0319-14-04: 30 µl Pct Recovery = 50% Analysis Date = 07/13/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 61% Analysis Date = 06/28/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 86% Analysis Date = 05/30/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 101% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 82% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-08: 20 µl & ERA 0406-15-09: 20 µl Pct Recovery = 64% Analysis Date = 11/24/15 SpikeMix = ERA 0406-15-09: 20 µl & Abs 050115: 20 µl Pct Recovery = 73% Analysis Date = 02/23/16 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 130% Analysis Date = 11/24/15 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 58% Analysis Date = 08/27/15 SpikeMix = Abs 052215: 20 µl & Abs 050115: 20 µl Pct Recovery = 58% Analysis Date = 07/09/15 SpikeMix = Abs 050115: 20 µl & Abs 052215: 20 µl Pct Recovery = 67% Analysis Date = 06/26/15 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 78% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 85% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 82% Analysis Date = 01/19/17 Pct Recovery = 73% Analysis Date = 01/14/17 Pct Recovery = 73% Analysis Date = 01/14/17 Pct Recovery = 73% Analysis Date = 01/09/17 Pct Recovery = 73% Analysis Date = 01/09/17 Pct Recovery = 73% Analysis Date = 01/04/17 Pct Recovery = 73% Analysis Date = 01/04/17 Pct Recovery = 73% Analysis Date = 12/30/16 Pct Recovery = 73% Analysis Date = 12/30/16 Pct Recovery = 73% Analysis Date = 12/25/16 Pct Recovery = 73% Analysis Date = 12/25/16 Pct Recovery = 73% Analysis Date = 12/21/16 Pct Recovery = 73% Analysis Date = 12/21/16 Pct Recovery = 73% Analysis Date = 12/16/16 Pct Recovery = 73% Analysis Date = 12/16/16 Pct Recovery = 73% Analysis Date = 12/11/16 Pct Recovery = 73% Analysis Date = 12/11/16 Pct Recovery = 73% Analysis Date = 12/06/16 Pct Recovery = 73% Analysis Date = 12/06/16 Pct Recovery = 73% Analysis Date = 12/01/16 Pct Recovery = 73% Analysis Date = 12/01/16 Pct Recovery = 73% Analysis Date = 11/26/16 Pct Recovery = 73% Analysis Date = 11/26/16 Pct Recovery = 73% Analysis Date = 11/22/16 Pct Recovery = 73% Analysis Date = 11/22/16 Pct Recovery = 73% Analysis Date = 11/17/16 Pct Recovery = 73% Analysis Date = 11/17/16 Pct Recovery = 73% Analysis Date = 11/12/16 Pct Recovery = 73% Analysis Date = 11/12/16 Pct Recovery = 73% Analysis Date = 11/07/16 Pct Recovery = 73% Analysis Date = 11/07/16 Pct Recovery = 73% Analysis Date = 11/02/16 Pct Recovery = 73% Analysis Date = 11/02/16 Pct Recovery = 73% Analysis Date = 10/28/16 Pct Recovery = 73% Analysis Date = 10/28/16 Pct Recovery = 73% Analysis Date = 10/24/16 Pct Recovery = 74% Analysis Date = 10/24/16 Pct Recovery = 74% Analysis Date = 10/19/16 Pct Recovery = 74% Analysis Date = 10/19/16 Pct Recovery = 74% Analysis Date = 10/14/16 Pct Recovery = 74% Analysis Date = 10/14/16 Pct Recovery = 74% Analysis Date = 10/09/16 Pct Recovery = 74% Analysis Date = 10/09/16 Pct Recovery = 74% Analysis Date = 10/04/16 Pct Recovery = 74% Analysis Date = 10/04/16 Pct Recovery = 74% Analysis Date = 09/30/16 Pct Recovery = 74% Analysis Date = 09/30/16 Pct Recovery = 74% Analysis Date = 09/25/16 Pct Recovery = 74% Analysis Date = 09/25/16 Pct Recovery = 74% Analysis Date = 09/20/16 Pct Recovery = 74% Analysis Date = 09/20/16 Pct Recovery = 74% Analysis Date = 09/15/16 Pct Recovery = 75% Analysis Date = 09/15/16 Pct Recovery = 75% Analysis Date = 09/10/16 Pct Recovery = 75% Analysis Date = 09/10/16 Pct Recovery = 75% Analysis Date = 09/05/16 Pct Recovery = 75% Analysis Date = 09/05/16 Pct Recovery = 75% Analysis Date = 09/01/16 Pct Recovery = 75% Analysis Date = 09/01/16 Pct Recovery = 75% Analysis Date = 08/27/16 Pct Recovery = 75% Analysis Date = 08/27/16 Pct Recovery = 75% Analysis Date = 08/22/16 Pct Recovery = 75% Analysis Date = 08/22/16 Pct Recovery = 75% Analysis Date = 08/17/16 Pct Recovery = 75% Analysis Date = 08/17/16 Pct Recovery = 75% Analysis Date = 08/12/16 Pct Recovery = 76% Analysis Date = 08/12/16 Pct Recovery = 76% Analysis Date = 08/07/16 Pct Recovery = 76% Analysis Date = 08/07/16 Pct Recovery = 76% Analysis Date = 08/03/16 Pct Recovery = 76% Analysis Date = 08/03/16 Pct Recovery = 76% Analysis Date = 07/29/16 Pct Recovery = 76% Analysis Date = 07/29/16 Pct Recovery = 76% Analysis Date = 07/24/16 Pct Recovery = 76% Analysis Date = 07/24/16 Pct Recovery = 76% Analysis Date = 07/19/16 Pct Recovery = 76% Analysis Date = 07/19/16 Pct Recovery = 76% Analysis Date = 07/14/16 Pct Recovery = 76% Analysis Date = 07/14/16 Pct Recovery = 76% Analysis Date = 07/10/16 Pct Recovery = 76% Analysis Date = 07/10/16 Pct Recovery = 76% Analysis Date = 07/05/16 Pct Recovery = 77% Analysis Date = 07/05/16 Pct Recovery = 77% Analysis Date = 06/30/16 Pct Recovery = 77% Analysis Date = 06/30/16 Pct Recovery = 77% Analysis Date = 06/25/16 Pct Recovery = 77% Analysis Date = 06/25/16 Pct Recovery = 77% Analysis Date = 06/20/16 Pct Recovery = 77% Analysis Date = 06/20/16 Pct Recovery = 77% Analysis Date = 06/15/16 Pct Recovery = 77% Analysis Date = 06/15/16 Pct Recovery = 77% Analysis Date = 06/11/16 Pct Recovery = 77% Analysis Date = 06/11/16 Pct Recovery = 77% Analysis Date = 06/06/16 Pct Recovery = 77% Analysis Date = 06/06/16 Pct Recovery = 77% Analysis Date = 06/01/16 Pct Recovery = 77% Analysis Date = 06/01/16 Pct Recovery = 77% Analysis Date = 05/27/16 Pct Recovery = 77% Analysis Date = 05/27/16 Pct Recovery = 77% Analysis Date = 05/22/16 Pct Recovery = 77% Analysis Date = 05/22/16 Pct Recovery = 77% Analysis Date = 05/17/16 Pct Recovery = 77% Analysis Date = 05/17/16 Pct Recovery = 77% Analysis Date = 05/13/16 Pct Recovery = 77% Analysis Date = 05/13/16 Pct Recovery = 77% Analysis Date = 05/08/16 Pct Recovery = 77% Analysis Date = 05/08/16 Pct Recovery = 77% Analysis Date = 05/03/16 Pct Recovery = 77% Analysis Date = 05/03/16 Pct Recovery = 77% Analysis Date = 04/28/16 Pct Recovery = 77% Analysis Date = 04/28/16 Pct Recovery = 77% Analysis Date = 04/23/16 Pct Recovery = 77% Analysis Date = 04/23/16 Pct Recovery = 77% Analysis Date = 04/18/16 Pct Recovery = 77% Analysis Date = 04/18/16 Pct Recovery = 77% Analysis Date = 04/14/16 Pct Recovery = 77% Analysis Date = 04/14/16 Pct Recovery = 77% Analysis Date = 04/09/16 Pct Recovery = 77% Analysis Date = 04/09/16 Pct Recovery = 77% Analysis Date = 04/04/16 Pct Recovery = 77% Analysis Date = 04/04/16 Pct Recovery = 77% Analysis Date = 03/30/16 Pct Recovery = 77% Analysis Date = 03/30/16 Pct Recovery = 77% Analysis Date = 03/25/16 Pct Recovery = 77% Analysis Date = 03/25/16 Pct Recovery = 77% Analysis Date = 03/21/16 Pct Recovery = 78% Analysis Date = 03/21/16 Pct Recovery = 78% Analysis Date = 03/16/16 Pct Recovery = 78% Analysis Date = 03/16/16 Pct Recovery = 78% Analysis Date = 03/11/16 Pct Recovery = 78% Analysis Date = 03/11/16 Pct Recovery = 78% Analysis Date = 03/06/16 Pct Recovery = 78% Analysis Date = 03/06/16 Pct Recovery = 78% Analysis Date = 03/01/16 Pct Recovery = 78% Analysis Date = 03/01/16 Pct Recovery = 78% Analysis Date = 02/25/16 Pct Recovery = 78% Analysis Date = 02/25/16 Pct Recovery = 78% Analysis Date = 02/21/16 Pct Recovery = 78% Analysis Date = 02/21/16 Pct Recovery = 78% Analysis Date = 02/16/16 Pct Recovery = 78% Analysis Date = 02/16/16 Pct Recovery = 78% Analysis Date = 02/11/16 Pct Recovery = 78% Analysis Date = 02/11/16 Pct Recovery = 78% Analysis Date = 02/06/16 Pct Recovery = 78% Analysis Date = 02/06/16 Pct Recovery = 78% Analysis Date = 02/01/16 Pct Recovery = 78% Analysis Date = 02/01/16 Pct Recovery = 78% Analysis Date = 01/27/16 Pct Recovery = 78% Analysis Date = 01/27/16 Pct Recovery = 78% Analysis Date = 01/23/16 Pct Recovery = 78% Analysis Date = 01/23/16 Pct Recovery = 78% Analysis Date = 01/18/16 Pct Recovery = 78% Analysis Date = 01/18/16 Pct Recovery = 78% Analysis Date = 01/13/16 Pct Recovery = 78% Analysis Date = 01/13/16 Pct Recovery = 78% Analysis Date = 01/08/16 Pct Recovery = 78% Analysis Date = 01/08/16 Pct Recovery = 78% Analysis Date = 01/03/16 Pct Recovery = 78% Analysis Date = 01/03/16 Pct Recovery = 78% Analysis Date = 12/30/15 Pct Recovery = 77% Analysis Date = 12/30/15 Pct Recovery = 77% Analysis Date = 12/25/15 Pct Recovery = 77% Analysis Date = 12/25/15 Pct Recovery = 77% Analysis Date = 12/20/15 Pct Recovery = 77% Analysis Date = 12/20/15 Pct Recovery = 77% Analysis Date = 12/15/15 Pct Recovery = 77% Analysis Date = 12/15/15 Pct Recovery = 77% Analysis Date = 12/10/15 Pct Recovery = 77% Analysis Date = 12/10/15 Pct Recovery = 77% Analysis Date = 12/05/15 Pct Recovery = 77% Analysis Date = 12/05/15 Pct Recovery = 77% Analysis Date = 12/01/15 Pct Recovery = 77% Analysis Date = 12/01/15 Pct Recovery = 77% Analysis Date = 11/26/15 Pct Recovery = 77% Analysis Date = 11/26/15 Pct Recovery = 77% Analysis Date = 11/21/15 Pct Recovery = 77% Analysis Date = 11/21/15 Pct Recovery = 77% Analysis Date = 11/16/15 Pct Recovery = 77% Analysis Date = 11/16/15 Pct Recovery = 77% Analysis Date = 11/11/15 Pct Recovery = 77% Analysis Date = 11/11/15 Pct Recovery = 77% Analysis Date = 11/06/15 Pct Recovery = 77% Analysis Date = 11/06/15 Pct Recovery = 77% Analysis Date = 11/02/15 Pct Recovery = 77% Analysis Date = 11/02/15 Pct Recovery = 77% Analysis Date = 10/28/15 Pct Recovery = 77% Analysis Date = 10/28/15 Pct Recovery = 77% Analysis Date = 10/23/15 Pct Recovery = 76% Analysis Date = 10/23/15 Pct Recovery = 76% Analysis Date = 10/18/15 Pct Recovery = 76% Analysis Date = 10/18/15 Pct Recovery = 76% Analysis Date = 10/13/15 Pct Recovery = 76% Analysis Date = 10/13/15 Pct Recovery = 76% Analysis Date = 10/08/15 Pct Recovery = 76% Analysis Date = 10/08/15 Pct Recovery = 76% Analysis Date = 10/04/15 Pct Recovery = 76% Analysis Date = 10/04/15 Pct Recovery = 76% Analysis Date = 09/29/15 Pct Recovery = 76% Analysis Date = 09/29/15 Pct Recovery = 76% Analysis Date = 09/24/15 Pct Recovery = 76% Analysis Date = 09/24/15 Pct Recovery = 76% Analysis Date = 09/19/15 Pct Recovery = 76% Analysis Date = 09/19/15 Pct Recovery = 76% Analysis Date = 09/14/15 Pct Recovery = 75% Analysis Date = 09/14/15 Pct Recovery = 75% Analysis Date = 09/10/15 Pct Recovery = 75% Analysis Date = 09/10/15 Pct Recovery = 75% Analysis Date = 09/05/15 Pct Recovery = 75% Analysis Date = 09/05/15 Pct Recovery = 75% Analysis Date = 08/31/15 Pct Recovery = 75% Analysis Date = 08/31/15 Pct Recovery = 75% Analysis Date = 08/26/15 Pct Recovery = 75% Analysis Date = 08/26/15 Pct Recovery = 75% Analysis Date = 08/21/15 Pct Recovery = 75% Analysis Date = 08/21/15 Pct Recovery = 75% Analysis Date = 08/16/15 Pct Recovery = 75% Analysis Date = 08/16/15 Pct Recovery = 75% Analysis Date = 08/12/15 Pct Recovery = 75% Analysis Date = 08/12/15 Pct Recovery = 75% Analysis Date = 08/07/15 Pct Recovery = 74% Analysis Date = 08/07/15 Pct Recovery = 74% Analysis Date = 08/02/15 Pct Recovery = 74% Analysis Date = 08/02/15 Pct Recovery = 74% Analysis Date = 07/28/15 Pct Recovery = 74% Analysis Date = 07/28/15 Pct Recovery = 74% Analysis Date = 07/23/15 Pct Recovery = 74% Analysis Date = 07/23/15 Pct Recovery = 74% Analysis Date = 07/18/15 Pct Recovery = 74% Analysis Date = 07/18/15 Pct Recovery = 74% Analysis Date = 07/14/15 Pct Recovery = 73% Analysis Date = 07/14/15 Pct Recovery = 73% Analysis Date = 07/09/15 Pct Recovery = 73% Analysis Date = 07/09/15 Pct Recovery = 73% Analysis Date = 07/04/15 Pct Recovery = 73% Analysis Date = 07/04/15 Pct Recovery = 73% Analysis Date = 06/29/15 Pct Recovery = 73% Analysis Date = 06/29/15 Pct Recovery = 73% Analysis Date = 06/24/15 Pct Recovery = 72% Analysis Date = 06/24/15 Pct Recovery = 72% Analysis Date = 06/20/15 Pct Recovery = 72% Analysis Date = 06/20/15 Pct Recovery = 72% Analysis Date = 06/15/15 Pct Recovery = 72% Analysis Date = 06/15/15 Pct Recovery = 72% Analysis Date = 06/10/15 Pct Recovery = 72% Analysis Date = 06/10/15 Pct Recovery = 72% Analysis Date = 06/05/15 Pct Recovery = 72% Analysis Date = 06/05/15 Pct Recovery = 72% Analysis Date = 05/31/15 Pct Recovery = 71% Analysis Date = 05/31/15 Pct Recovery = 71% Analysis Date = 05/26/15 Pct Recovery = 71% Analysis Date = 05/26/15 Pct Recovery = 71% Analysis Date = 05/22/15 Pct Recovery = 71% Analysis Date = 05/22/15 Pct Recovery = 71% Analysis Date = 05/17/15 Pct Recovery = 71% Analysis Date = 05/17/15 Pct Recovery = 71% Analysis Date = 05/12/15 Pct Recovery = 70% Analysis Date = 05/12/15 Pct Recovery = 70% Analysis Date = 05/07/15 Pct Recovery = 70% Analysis Date = 05/07/15 Pct Recovery = 70% Analysis Date = 05/02/15 Pct Recovery = 70% Analysis Date = 05/02/15 Pct Recovery = 70% Analysis Date = 04/27/15 Pct Recovery = 70% Analysis Date = 04/27/15 Pct Recovery = 70% Analysis Date = 04/23/15 Pct Recovery = 70% Analysis Date = 04/23/15 Pct Recovery = 70% Analysis Date = 04/18/15 Pct Recovery = 70% Analysis Date = 04/18/15 Pct Recovery = 70% Analysis Date = 04/13/15 Pct Recovery = 70% Analysis Date = 04/13/15 Pct Recovery = 70% Analysis Date = 04/08/15 Pct Recovery = 70% Analysis Date = 04/08/15 Pct Recovery = 70% Analysis Date = 04/03/15 Pct Recovery = 70% Analysis Date = 04/03/15 Pct Recovery = 70% Analysis Date = 03/29/15 Pct Recovery = 70% Analysis Date = 03/29/15 Pct Recovery = 70% Analysis Date = 03/25/15 Pct Recovery = 70% Analysis Date = 03/25/15 Pct Recovery = 70% Analysis Date = 03/20/15 Pct Recovery = 70% Analysis Date = 03/20/15 Pct Recovery = 70% Analysis Date = 03/15/15 Pct Recovery = 70% Analysis Date = 03/15/15 Pct Recovery = 70% Analysis Date = 03/10/15 Pct Recovery = 70% Analysis Date = 03/10/15 Pct Recovery = 70% Analysis Date = 03/05/15 Pct Recovery = 70% Analysis Date = 03/05/15 Pct Recovery = 70% Analysis Date = 03/01/15 Pct Recovery = 71% Analysis Date = 03/01/15 Pct Recovery = 71% Analysis Date = 02/24/15 Pct Recovery = 71% Analysis Date = 02/24/15 Pct Recovery = 71% Analysis Date = 02/19/15 Pct Recovery = 71% Analysis Date = 02/19/15 Pct Recovery = 71% Analysis Date = 02/14/15 Pct Recovery = 71% Analysis Date = 02/14/15 Pct Recovery = 71% Analysis Date = 02/09/15 Pct Recovery = 71% Analysis Date = 02/09/15 Pct Recovery = 71% Analysis Date = 02/04/15 Pct Recovery = 71% Analysis Date = 02/04/15 Pct Recovery = 71% Analysis Date = 01/31/15 Pct Recovery = 71% Analysis Date = 01/31/15 Pct Recovery = 71% Analysis Date = 01/26/15 Pct Recovery = 71% Analysis Date = 01/26/15 Pct Recovery = 71% Analysis Date = 01/21/15 Pct Recovery = 71% Analysis Date = 01/21/15 Pct Recovery = 71% Analysis Date = 01/16/15 Pct Recovery = 71% Analysis Date = 01/16/15 Pct Recovery = 71% Analysis Date = 01/11/15 Pct Recovery = 71% Analysis Date = 01/11/15 Pct Recovery = 71% Analysis Date = 01/06/15 Pct Recovery = 71% Analysis Date = 01/06/15 Pct Recovery = 71% Analysis Date = 01/02/15 Pct Recovery = 71% Analysis Date = 01/02/15 Pct Recovery = 71% Analysis Date = 12/28/14 Pct Recovery = 71% Analysis Date = 12/28/14 Pct Recovery = 71% Analysis Date = 12/23/14 Pct Recovery = 71% Analysis Date = 12/23/14 Pct Recovery = 71% Analysis Date = 12/18/14 Pct Recovery = 72% Analysis Date = 12/18/14 Pct Recovery = 72% Analysis Date = 12/13/14 Pct Recovery = 72% Analysis Date = 12/13/14 Pct Recovery = 72% Analysis Date = 12/09/14 Pct Recovery = 72% Analysis Date = 12/09/14 Pct Recovery = 72% Analysis Date = 12/04/14 Pct Recovery = 72% Analysis Date = 12/04/14 Pct Recovery = 72% Analysis Date = 11/29/14 Pct Recovery = 72% Analysis Date = 11/29/14 Pct Recovery = 72% Analysis Date = 11/24/14 Pct Recovery = 72% Analysis Date = 11/24/14 Pct Recovery = 72% Analysis Date = 11/19/14 Pct Recovery = 72% Analysis Date = 11/19/14 Pct Recovery = 72% Analysis Date = 11/14/14 Pct Recovery = 72% Analysis Date = 11/14/14 Pct Recovery = 72% Analysis Date = 11/10/14 Pct Recovery = 72% Analysis Date = 11/10/14 Pct Recovery = 72% Analysis Date = 11/05/14 Pct Recovery = 72% Analysis Date = 11/05/14 Pct Recovery = 72% Analysis Date = 10/31/14 Pct Recovery = 72% Analysis Date = 10/31/14 Pct Recovery = 72% Analysis Date = 10/26/14 Pct Recovery = 72% Analysis Date = 10/26/14 Pct Recovery = 72% Analysis Date = 10/21/14 Pct Recovery = 72% Analysis Date = 10/21/14 Pct Recovery = 72% Analysis Date = 10/16/14 Pct Recovery = 72% Analysis Date = 10/16/14 Pct Recovery = 72% Analysis Date = 10/12/14 Pct Recovery = 73% Analysis Date = 10/12/14 Pct Recovery = 73% Analysis Date = 10/07/14 Pct Recovery = 73% Analysis Date = 10/07/14 Pct Recovery = 73% Analysis Date = 10/02/14 Pct Recovery = 73% Analysis Date = 10/02/14 Pct Recovery = 73% Analysis Date = 09/27/14 Pct Recovery = 73% Analysis Date = 09/27/14 Pct Recovery = 73% Analysis Date = 09/22/14 Pct Recovery = 73% Analysis Date = 09/22/14 Pct Recovery = 73% Analysis Date = 09/17/14 Pct Recovery = 73% Analysis Date = 09/17/14 Pct Recovery = 73% Analysis Date = 09/13/14 Pct Recovery = 73% Analysis Date = 09/13/14 Pct Recovery = 73% Analysis Date = 09/08/14 Pct Recovery = 73% Analysis Date = 09/08/14 Pct Recovery = 73% Analysis Date = 09/03/14 Pct Recovery = 73% Analysis Date = 09/03/14 Pct Recovery = 73% Analysis Date = 08/29/14 Pct Recovery = 73% Analysis Date = 08/29/14 Pct Recovery = 73% Analysis Date = 08/24/14 Pct Recovery = 73% Analysis Date = 08/24/14 Pct Recovery = 73% Analysis Date = 08/20/14 Pct Recovery = 73% Analysis Date = 08/20/14 Pct Recovery = 73% Analysis Date = 08/15/14 Pct Recovery = 73% Analysis Date = 08/15/14 Pct Recovery = 73% Analysis Date = 08/10/14 Pct Recovery = 74% Analysis Date = 08/10/14 Pct Recovery = 74% Analysis Date = 08/05/14 Pct Recovery = 74% Analysis Date = 08/05/14 Pct Recovery = 74% Analysis Date = 07/31/14 Pct Recovery = 74% Analysis Date = 07/31/14 Pct Recovery = 74% Analysis Date = 07/26/14 Pct Recovery = 74% Analysis Date = 07/26/14 Pct Recovery = 74% Analysis Date = 07/22/14 Pct Recovery = 74% Analysis Date = 07/22/14 Pct Recovery = 74% Analysis Date = 07/17/14 Pct Recovery = 74% Analysis Date = 07/17/14 Pct Recovery = 74% Analysis Date = 07/12/14 Pct Recovery = 74% Analysis Date = 07/12/14 Pct Recovery = 74% Analysis Date = 07/07/14 Pct Recovery = 74% Analysis Date = 07/07/14 Pct Recovery = 74% Analysis Date = 07/02/14 Pct Recovery = 74% Analysis Date = 07/02/14 Pct Recovery = 74% Analysis Date = 06/27/14 Pct Recovery = 74% Analysis Date = 06/27/14 Pct Recovery = 74% Analysis Date = 06/23/14 Pct Recovery = 74% Analysis Date = 06/23/14 Pct Recovery = 74% Analysis Date = 06/18/14 Pct Recovery = 75% Analysis Date = 06/18/14 Pct Recovery = 75% Analysis Date = 06/13/14 Pct Recovery = 75% Analysis Date = 06/13/14 Pct Recovery = 75% Analysis Date = 06/08/14 Pct Recovery = 75% Analysis Date = 06/08/14 Pct Recovery = 75% Analysis Date = 06/03/14 Pct Recovery = 75% Analysis Date = 06/03/14 Pct Recovery = 75% Analysis Date = 05/30/14 Pct Recovery = 75% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
THIABENDAZOLE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 2 83% 2% 83% 2%
>= Reporting Level 57 74% 19% 74% 12%
Total 59 74% 19% 74% 13%

Sample Statistics
THIABENDAZOLE

Characteristic N % % Basis
Plotted 59 79% Spiked
Estimated Values 20 27% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 4 5% Spiked
Spiked 75 .  
False Negatives 12 16% 12 out of 75
Not Spiked 40 .  
False Positives 0 0% 0 out of 40

BQS OBSP Determination:
TIOTROPIUM
METHOD: 2440 , TESTIDCODE: 67508LCM56
Open Data Set

Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 15% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 17% Analysis Date = 01/17/16 SpikeMix = ERA 0406-15-09: 80 µl & ERA 0406-15-07A: 80 µl Pct Recovery = 76% Analysis Date = 11/24/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 60% Analysis Date = 11/05/15 SpikeMix = ERA 0406-15-08: 80 µl & Abs 052215: 80 µl Pct Recovery = 14% Analysis Date = 11/04/15 SpikeMix = Abs 052215: 80 µl & Abs 050115: 80 µl Pct Recovery = 21% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 18% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 30% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 23% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 23% Analysis Date = 04/29/15 SpikeMix = ERA 0319-14-05: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 34% Analysis Date = 03/11/15 SpikeMix = ERA 0318-14-02: 15 µl & Abs 041714: 15 µl Pct Recovery = 55% Analysis Date = 02/06/15 SpikeMix = Abs 041814: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 39% Analysis Date = 12/06/14 SpikeMix = ERA 0318-14-02: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 26% Analysis Date = 10/11/14 SpikeMix = ERA 0318-14-02: 60 µl & ERA 0319-14-04: 60 µl Pct Recovery = 10% Analysis Date = 07/26/14 SpikeMix = ERA 0319-14-05: 60 µl & ERA 0318-14-02: 60 µl Pct Recovery = 6% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-08: 40 µl & ERA 0406-15-09: 40 µl Pct Recovery = 60% Analysis Date = 07/31/15 SpikeMix = ERA 0406-15-09: 40 µl & Abs 050115: 40 µl Pct Recovery = 49% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-08: 40 µl & Abs 052215: 40 µl Pct Recovery = 32% Analysis Date = 02/23/16 SpikeMix = Abs 052215: 40 µl & Abs 050115: 40 µl Pct Recovery = 16% Analysis Date = 09/10/15 SpikeMix = Abs 052215: 40 µl & ERA 0406-15-07A: 40 µl Pct Recovery = 19% Analysis Date = 07/31/15 SpikeMix = Abs 051315: 40 µl & Abs 052215: 40 µl Pct Recovery = 16% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 7% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 16% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 55% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 53% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 3% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 4% Analysis Date = 12/07/14 SpikeMix = ERA 0318-14-02: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 50% Analysis Date = 11/04/14 SpikeMix = Abs 041814: 8 µl & ERA 0318-14-02: 8 µl Pct Recovery = 53% Analysis Date = 08/30/14 SpikeMix = ERA 0318-14-02: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 14% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 45% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 23% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-08: 20 µl & ERA 0406-15-09: 20 µl Pct Recovery = 52% Analysis Date = 11/24/15 SpikeMix = ERA 0406-15-09: 20 µl & Abs 050115: 20 µl Pct Recovery = 42% Analysis Date = 02/23/16 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 29% Analysis Date = 11/24/15 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 28% Analysis Date = 09/09/15 SpikeMix = ERA 0406-15-08: 20 µl & Abs 052215: 20 µl Pct Recovery = 6% Analysis Date = 08/27/15 SpikeMix = Abs 052215: 20 µl & Abs 050115: 20 µl Pct Recovery = 32% Analysis Date = 07/09/15 SpikeMix = Abs 050115: 20 µl & Abs 052215: 20 µl Pct Recovery = 34% Analysis Date = 06/26/15 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 160% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 36% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 32% Analysis Date = 04/09/16 SpikeMix = Abs 051315: 10 µl & ERA 0406-15-09: 10 µl Pct Recovery = 31% Analysis Date = 01/19/17 Pct Recovery = 19% Analysis Date = 01/14/17 Pct Recovery = 19% Analysis Date = 01/14/17 Pct Recovery = 19% Analysis Date = 01/09/17 Pct Recovery = 20% Analysis Date = 01/09/17 Pct Recovery = 20% Analysis Date = 01/05/17 Pct Recovery = 20% Analysis Date = 01/05/17 Pct Recovery = 20% Analysis Date = 12/31/16 Pct Recovery = 20% Analysis Date = 12/31/16 Pct Recovery = 20% Analysis Date = 12/27/16 Pct Recovery = 20% Analysis Date = 12/27/16 Pct Recovery = 20% Analysis Date = 12/22/16 Pct Recovery = 20% Analysis Date = 12/22/16 Pct Recovery = 20% Analysis Date = 12/18/16 Pct Recovery = 21% Analysis Date = 12/18/16 Pct Recovery = 21% Analysis Date = 12/13/16 Pct Recovery = 21% Analysis Date = 12/13/16 Pct Recovery = 21% Analysis Date = 12/09/16 Pct Recovery = 21% Analysis Date = 12/09/16 Pct Recovery = 21% Analysis Date = 12/04/16 Pct Recovery = 21% Analysis Date = 12/04/16 Pct Recovery = 21% Analysis Date = 11/30/16 Pct Recovery = 21% Analysis Date = 11/30/16 Pct Recovery = 21% Analysis Date = 11/25/16 Pct Recovery = 21% Analysis Date = 11/25/16 Pct Recovery = 21% Analysis Date = 11/20/16 Pct Recovery = 22% Analysis Date = 11/20/16 Pct Recovery = 22% Analysis Date = 11/16/16 Pct Recovery = 22% Analysis Date = 11/16/16 Pct Recovery = 22% Analysis Date = 11/11/16 Pct Recovery = 22% Analysis Date = 11/11/16 Pct Recovery = 22% Analysis Date = 11/07/16 Pct Recovery = 22% Analysis Date = 11/07/16 Pct Recovery = 22% Analysis Date = 11/02/16 Pct Recovery = 22% Analysis Date = 11/02/16 Pct Recovery = 22% Analysis Date = 10/29/16 Pct Recovery = 23% Analysis Date = 10/29/16 Pct Recovery = 23% Analysis Date = 10/24/16 Pct Recovery = 23% Analysis Date = 10/24/16 Pct Recovery = 23% Analysis Date = 10/20/16 Pct Recovery = 23% Analysis Date = 10/20/16 Pct Recovery = 23% Analysis Date = 10/15/16 Pct Recovery = 23% Analysis Date = 10/15/16 Pct Recovery = 23% Analysis Date = 10/11/16 Pct Recovery = 23% Analysis Date = 10/11/16 Pct Recovery = 23% Analysis Date = 10/06/16 Pct Recovery = 24% Analysis Date = 10/06/16 Pct Recovery = 24% Analysis Date = 10/02/16 Pct Recovery = 24% Analysis Date = 10/02/16 Pct Recovery = 24% Analysis Date = 09/27/16 Pct Recovery = 24% Analysis Date = 09/27/16 Pct Recovery = 24% Analysis Date = 09/22/16 Pct Recovery = 24% Analysis Date = 09/22/16 Pct Recovery = 24% Analysis Date = 09/18/16 Pct Recovery = 24% Analysis Date = 09/18/16 Pct Recovery = 24% Analysis Date = 09/13/16 Pct Recovery = 24% Analysis Date = 09/13/16 Pct Recovery = 24% Analysis Date = 09/09/16 Pct Recovery = 25% Analysis Date = 09/09/16 Pct Recovery = 25% Analysis Date = 09/04/16 Pct Recovery = 25% Analysis Date = 09/04/16 Pct Recovery = 25% Analysis Date = 08/31/16 Pct Recovery = 25% Analysis Date = 08/31/16 Pct Recovery = 25% Analysis Date = 08/26/16 Pct Recovery = 25% Analysis Date = 08/26/16 Pct Recovery = 25% Analysis Date = 08/22/16 Pct Recovery = 25% Analysis Date = 08/22/16 Pct Recovery = 25% Analysis Date = 08/17/16 Pct Recovery = 26% Analysis Date = 08/17/16 Pct Recovery = 26% Analysis Date = 08/13/16 Pct Recovery = 26% Analysis Date = 08/13/16 Pct Recovery = 26% Analysis Date = 08/08/16 Pct Recovery = 26% Analysis Date = 08/08/16 Pct Recovery = 26% Analysis Date = 08/04/16 Pct Recovery = 26% Analysis Date = 08/04/16 Pct Recovery = 26% Analysis Date = 07/30/16 Pct Recovery = 27% Analysis Date = 07/30/16 Pct Recovery = 27% Analysis Date = 07/25/16 Pct Recovery = 27% Analysis Date = 07/25/16 Pct Recovery = 27% Analysis Date = 07/21/16 Pct Recovery = 27% Analysis Date = 07/21/16 Pct Recovery = 27% Analysis Date = 07/16/16 Pct Recovery = 27% Analysis Date = 07/16/16 Pct Recovery = 27% Analysis Date = 07/12/16 Pct Recovery = 28% Analysis Date = 07/12/16 Pct Recovery = 28% Analysis Date = 07/07/16 Pct Recovery = 28% Analysis Date = 07/07/16 Pct Recovery = 28% Analysis Date = 07/03/16 Pct Recovery = 28% Analysis Date = 07/03/16 Pct Recovery = 28% Analysis Date = 06/28/16 Pct Recovery = 28% Analysis Date = 06/28/16 Pct Recovery = 28% Analysis Date = 06/24/16 Pct Recovery = 29% Analysis Date = 06/24/16 Pct Recovery = 29% Analysis Date = 06/19/16 Pct Recovery = 29% Analysis Date = 06/19/16 Pct Recovery = 29% Analysis Date = 06/15/16 Pct Recovery = 29% Analysis Date = 06/15/16 Pct Recovery = 29% Analysis Date = 06/10/16 Pct Recovery = 29% Analysis Date = 06/10/16 Pct Recovery = 29% Analysis Date = 06/06/16 Pct Recovery = 30% Analysis Date = 06/06/16 Pct Recovery = 30% Analysis Date = 06/01/16 Pct Recovery = 30% Analysis Date = 06/01/16 Pct Recovery = 30% Analysis Date = 05/27/16 Pct Recovery = 30% Analysis Date = 05/27/16 Pct Recovery = 30% Analysis Date = 05/23/16 Pct Recovery = 30% Analysis Date = 05/23/16 Pct Recovery = 30% Analysis Date = 05/18/16 Pct Recovery = 31% Analysis Date = 05/18/16 Pct Recovery = 31% Analysis Date = 05/14/16 Pct Recovery = 31% Analysis Date = 05/14/16 Pct Recovery = 31% Analysis Date = 05/09/16 Pct Recovery = 31% Analysis Date = 05/09/16 Pct Recovery = 31% Analysis Date = 05/05/16 Pct Recovery = 31% Analysis Date = 05/05/16 Pct Recovery = 31% Analysis Date = 04/30/16 Pct Recovery = 32% Analysis Date = 04/30/16 Pct Recovery = 32% Analysis Date = 04/26/16 Pct Recovery = 32% Analysis Date = 04/26/16 Pct Recovery = 32% Analysis Date = 04/21/16 Pct Recovery = 32% Analysis Date = 04/21/16 Pct Recovery = 32% Analysis Date = 04/17/16 Pct Recovery = 32% Analysis Date = 04/17/16 Pct Recovery = 32% Analysis Date = 04/12/16 Pct Recovery = 33% Analysis Date = 04/12/16 Pct Recovery = 33% Analysis Date = 04/07/16 Pct Recovery = 33% Analysis Date = 04/07/16 Pct Recovery = 33% Analysis Date = 04/03/16 Pct Recovery = 33% Analysis Date = 04/03/16 Pct Recovery = 33% Analysis Date = 03/29/16 Pct Recovery = 33% Analysis Date = 03/29/16 Pct Recovery = 33% Analysis Date = 03/25/16 Pct Recovery = 34% Analysis Date = 03/25/16 Pct Recovery = 34% Analysis Date = 03/20/16 Pct Recovery = 34% Analysis Date = 03/20/16 Pct Recovery = 34% Analysis Date = 03/16/16 Pct Recovery = 34% Analysis Date = 03/16/16 Pct Recovery = 34% Analysis Date = 03/11/16 Pct Recovery = 34% Analysis Date = 03/11/16 Pct Recovery = 34% Analysis Date = 03/07/16 Pct Recovery = 35% Analysis Date = 03/07/16 Pct Recovery = 35% Analysis Date = 03/02/16 Pct Recovery = 35% Analysis Date = 03/02/16 Pct Recovery = 35% Analysis Date = 02/27/16 Pct Recovery = 35% Analysis Date = 02/27/16 Pct Recovery = 35% Analysis Date = 02/22/16 Pct Recovery = 35% Analysis Date = 02/22/16 Pct Recovery = 35% Analysis Date = 02/18/16 Pct Recovery = 35% Analysis Date = 02/18/16 Pct Recovery = 35% Analysis Date = 02/13/16 Pct Recovery = 35% Analysis Date = 02/13/16 Pct Recovery = 35% Analysis Date = 02/08/16 Pct Recovery = 36% Analysis Date = 02/08/16 Pct Recovery = 36% Analysis Date = 02/04/16 Pct Recovery = 36% Analysis Date = 02/04/16 Pct Recovery = 36% Analysis Date = 01/30/16 Pct Recovery = 36% Analysis Date = 01/30/16 Pct Recovery = 36% Analysis Date = 01/26/16 Pct Recovery = 36% Analysis Date = 01/26/16 Pct Recovery = 36% Analysis Date = 01/21/16 Pct Recovery = 36% Analysis Date = 01/21/16 Pct Recovery = 36% Analysis Date = 01/17/16 Pct Recovery = 36% Analysis Date = 01/17/16 Pct Recovery = 36% Analysis Date = 01/12/16 Pct Recovery = 36% Analysis Date = 01/12/16 Pct Recovery = 36% Analysis Date = 01/08/16 Pct Recovery = 37% Analysis Date = 01/08/16 Pct Recovery = 37% Analysis Date = 01/03/16 Pct Recovery = 37% Analysis Date = 01/03/16 Pct Recovery = 37% Analysis Date = 12/30/15 Pct Recovery = 37% Analysis Date = 12/30/15 Pct Recovery = 37% Analysis Date = 12/25/15 Pct Recovery = 37% Analysis Date = 12/25/15 Pct Recovery = 37% Analysis Date = 12/21/15 Pct Recovery = 37% Analysis Date = 12/21/15 Pct Recovery = 37% Analysis Date = 12/16/15 Pct Recovery = 37% Analysis Date = 12/16/15 Pct Recovery = 37% Analysis Date = 12/11/15 Pct Recovery = 37% Analysis Date = 12/11/15 Pct Recovery = 37% Analysis Date = 12/07/15 Pct Recovery = 38% Analysis Date = 12/07/15 Pct Recovery = 38% Analysis Date = 12/02/15 Pct Recovery = 38% Analysis Date = 12/02/15 Pct Recovery = 38% Analysis Date = 11/28/15 Pct Recovery = 38% Analysis Date = 11/28/15 Pct Recovery = 38% Analysis Date = 11/23/15 Pct Recovery = 38% Analysis Date = 11/23/15 Pct Recovery = 38% Analysis Date = 11/19/15 Pct Recovery = 38% Analysis Date = 11/19/15 Pct Recovery = 38% Analysis Date = 11/14/15 Pct Recovery = 39% Analysis Date = 11/14/15 Pct Recovery = 39% Analysis Date = 11/10/15 Pct Recovery = 39% Analysis Date = 11/10/15 Pct Recovery = 39% Analysis Date = 11/05/15 Pct Recovery = 39% Analysis Date = 11/05/15 Pct Recovery = 39% Analysis Date = 11/01/15 Pct Recovery = 40% Analysis Date = 11/01/15 Pct Recovery = 40% Analysis Date = 10/27/15 Pct Recovery = 40% Analysis Date = 10/27/15 Pct Recovery = 40% Analysis Date = 10/23/15 Pct Recovery = 40% Analysis Date = 10/23/15 Pct Recovery = 40% Analysis Date = 10/18/15 Pct Recovery = 41% Analysis Date = 10/18/15 Pct Recovery = 41% Analysis Date = 10/13/15 Pct Recovery = 41% Analysis Date = 10/13/15 Pct Recovery = 41% Analysis Date = 10/09/15 Pct Recovery = 41% Analysis Date = 10/09/15 Pct Recovery = 41% Analysis Date = 10/04/15 Pct Recovery = 42% Analysis Date = 10/04/15 Pct Recovery = 42% Analysis Date = 09/30/15 Pct Recovery = 42% Analysis Date = 09/30/15 Pct Recovery = 42% Analysis Date = 09/25/15 Pct Recovery = 42% Analysis Date = 09/25/15 Pct Recovery = 42% Analysis Date = 09/21/15 Pct Recovery = 43% Analysis Date = 09/21/15 Pct Recovery = 43% Analysis Date = 09/16/15 Pct Recovery = 43% Analysis Date = 09/16/15 Pct Recovery = 43% Analysis Date = 09/12/15 Pct Recovery = 43% Analysis Date = 09/12/15 Pct Recovery = 43% Analysis Date = 09/07/15 Pct Recovery = 44% Analysis Date = 09/07/15 Pct Recovery = 44% Analysis Date = 09/03/15 Pct Recovery = 44% Analysis Date = 09/03/15 Pct Recovery = 44% Analysis Date = 08/29/15 Pct Recovery = 44% Analysis Date = 08/29/15 Pct Recovery = 44% Analysis Date = 08/24/15 Pct Recovery = 44% Analysis Date = 08/24/15 Pct Recovery = 44% Analysis Date = 08/20/15 Pct Recovery = 45% Analysis Date = 08/20/15 Pct Recovery = 45% Analysis Date = 08/15/15 Pct Recovery = 45% Analysis Date = 08/15/15 Pct Recovery = 45% Analysis Date = 08/11/15 Pct Recovery = 45% Analysis Date = 08/11/15 Pct Recovery = 45% Analysis Date = 08/06/15 Pct Recovery = 45% Analysis Date = 08/06/15 Pct Recovery = 45% Analysis Date = 08/02/15 Pct Recovery = 45% Analysis Date = 08/02/15 Pct Recovery = 45% Analysis Date = 07/28/15 Pct Recovery = 45% Analysis Date = 07/28/15 Pct Recovery = 45% Analysis Date = 07/24/15 Pct Recovery = 45% Analysis Date = 07/24/15 Pct Recovery = 45% Analysis Date = 07/19/15 Pct Recovery = 45% Analysis Date = 07/19/15 Pct Recovery = 45% Analysis Date = 07/15/15 Pct Recovery = 46% Analysis Date = 07/15/15 Pct Recovery = 46% Analysis Date = 07/10/15 Pct Recovery = 46% Analysis Date = 07/10/15 Pct Recovery = 46% Analysis Date = 07/06/15 Pct Recovery = 46% Analysis Date = 07/06/15 Pct Recovery = 46% Analysis Date = 07/01/15 Pct Recovery = 45% Analysis Date = 07/01/15 Pct Recovery = 45% Analysis Date = 06/26/15 Pct Recovery = 45% Analysis Date = 06/26/15 Pct Recovery = 45% Analysis Date = 06/22/15 Pct Recovery = 45% Analysis Date = 06/22/15 Pct Recovery = 45% Analysis Date = 06/17/15 Pct Recovery = 45% Analysis Date = 06/17/15 Pct Recovery = 45% Analysis Date = 06/13/15 Pct Recovery = 44% Analysis Date = 06/13/15 Pct Recovery = 44% Analysis Date = 06/08/15 Pct Recovery = 44% Analysis Date = 06/08/15 Pct Recovery = 44% Analysis Date = 06/04/15 Pct Recovery = 44% Analysis Date = 06/04/15 Pct Recovery = 44% Analysis Date = 05/30/15 Pct Recovery = 43% Analysis Date = 05/30/15 Pct Recovery = 43% Analysis Date = 05/26/15 Pct Recovery = 43% Analysis Date = 05/26/15 Pct Recovery = 43% Analysis Date = 05/21/15 Pct Recovery = 43% Analysis Date = 05/21/15 Pct Recovery = 43% Analysis Date = 05/17/15 Pct Recovery = 43% Analysis Date = 05/17/15 Pct Recovery = 43% Analysis Date = 05/12/15 Pct Recovery = 42% Analysis Date = 05/12/15 Pct Recovery = 42% Analysis Date = 05/08/15 Pct Recovery = 42% Analysis Date = 05/08/15 Pct Recovery = 42% Analysis Date = 05/03/15 Pct Recovery = 42% Analysis Date = 05/03/15 Pct Recovery = 42% Analysis Date = 04/28/15 Pct Recovery = 42% Analysis Date = 04/28/15 Pct Recovery = 42% Analysis Date = 04/24/15 Pct Recovery = 41% Analysis Date = 04/24/15 Pct Recovery = 41% Analysis Date = 04/19/15 Pct Recovery = 41% Analysis Date = 04/19/15 Pct Recovery = 41% Analysis Date = 04/15/15 Pct Recovery = 41% Analysis Date = 04/15/15 Pct Recovery = 41% Analysis Date = 04/10/15 Pct Recovery = 41% Analysis Date = 04/10/15 Pct Recovery = 41% Analysis Date = 04/06/15 Pct Recovery = 40% Analysis Date = 04/06/15 Pct Recovery = 40% Analysis Date = 04/01/15 Pct Recovery = 40% Analysis Date = 04/01/15 Pct Recovery = 40% Analysis Date = 03/28/15 Pct Recovery = 40% Analysis Date = 03/28/15 Pct Recovery = 40% Analysis Date = 03/23/15 Pct Recovery = 39% Analysis Date = 03/23/15 Pct Recovery = 39% Analysis Date = 03/19/15 Pct Recovery = 39% Analysis Date = 03/19/15 Pct Recovery = 39% Analysis Date = 03/14/15 Pct Recovery = 39% Analysis Date = 03/14/15 Pct Recovery = 39% Analysis Date = 03/10/15 Pct Recovery = 39% Analysis Date = 03/10/15 Pct Recovery = 39% Analysis Date = 03/05/15 Pct Recovery = 38% Analysis Date = 03/05/15 Pct Recovery = 38% Analysis Date = 02/28/15 Pct Recovery = 38% Analysis Date = 02/28/15 Pct Recovery = 38% Analysis Date = 02/24/15 Pct Recovery = 38% Analysis Date = 02/24/15 Pct Recovery = 38% Analysis Date = 02/19/15 Pct Recovery = 38% Analysis Date = 02/19/15 Pct Recovery = 38% Analysis Date = 02/15/15 Pct Recovery = 37% Analysis Date = 02/15/15 Pct Recovery = 37% Analysis Date = 02/10/15 Pct Recovery = 37% Analysis Date = 02/10/15 Pct Recovery = 37% Analysis Date = 02/06/15 Pct Recovery = 37% Analysis Date = 02/06/15 Pct Recovery = 37% Analysis Date = 02/01/15 Pct Recovery = 36% Analysis Date = 02/01/15 Pct Recovery = 36% Analysis Date = 01/28/15 Pct Recovery = 36% Analysis Date = 01/28/15 Pct Recovery = 36% Analysis Date = 01/23/15 Pct Recovery = 36% Analysis Date = 01/23/15 Pct Recovery = 36% Analysis Date = 01/19/15 Pct Recovery = 36% Analysis Date = 01/19/15 Pct Recovery = 36% Analysis Date = 01/14/15 Pct Recovery = 35% Analysis Date = 01/14/15 Pct Recovery = 35% Analysis Date = 01/09/15 Pct Recovery = 35% Analysis Date = 01/09/15 Pct Recovery = 35% Analysis Date = 01/05/15 Pct Recovery = 35% Analysis Date = 01/05/15 Pct Recovery = 35% Analysis Date = 12/31/14 Pct Recovery = 35% Analysis Date = 12/31/14 Pct Recovery = 35% Analysis Date = 12/27/14 Pct Recovery = 34% Analysis Date = 12/27/14 Pct Recovery = 34% Analysis Date = 12/22/14 Pct Recovery = 34% Analysis Date = 12/22/14 Pct Recovery = 34% Analysis Date = 12/18/14 Pct Recovery = 34% Analysis Date = 12/18/14 Pct Recovery = 34% Analysis Date = 12/13/14 Pct Recovery = 34% Analysis Date = 12/13/14 Pct Recovery = 34% Analysis Date = 12/09/14 Pct Recovery = 33% Analysis Date = 12/09/14 Pct Recovery = 33% Analysis Date = 12/04/14 Pct Recovery = 33% Analysis Date = 12/04/14 Pct Recovery = 33% Analysis Date = 11/30/14 Pct Recovery = 33% Analysis Date = 11/30/14 Pct Recovery = 33% Analysis Date = 11/25/14 Pct Recovery = 32% Analysis Date = 11/25/14 Pct Recovery = 32% Analysis Date = 11/21/14 Pct Recovery = 32% Analysis Date = 11/21/14 Pct Recovery = 32% Analysis Date = 11/16/14 Pct Recovery = 32% Analysis Date = 11/16/14 Pct Recovery = 32% Analysis Date = 11/11/14 Pct Recovery = 31% Analysis Date = 11/11/14 Pct Recovery = 31% Analysis Date = 11/07/14 Pct Recovery = 31% Analysis Date = 11/07/14 Pct Recovery = 31% Analysis Date = 11/02/14 Pct Recovery = 31% Analysis Date = 11/02/14 Pct Recovery = 31% Analysis Date = 10/29/14 Pct Recovery = 30% Analysis Date = 10/29/14 Pct Recovery = 30% Analysis Date = 10/24/14 Pct Recovery = 30% Analysis Date = 10/24/14 Pct Recovery = 30% Analysis Date = 10/20/14 Pct Recovery = 30% Analysis Date = 10/20/14 Pct Recovery = 30% Analysis Date = 10/15/14 Pct Recovery = 29% Analysis Date = 10/15/14 Pct Recovery = 29% Analysis Date = 10/11/14 Pct Recovery = 29% Analysis Date = 10/11/14 Pct Recovery = 29% Analysis Date = 10/06/14 Pct Recovery = 28% Analysis Date = 10/06/14 Pct Recovery = 28% Analysis Date = 10/02/14 Pct Recovery = 28% Analysis Date = 10/02/14 Pct Recovery = 28% Analysis Date = 09/27/14 Pct Recovery = 28% Analysis Date = 09/27/14 Pct Recovery = 28% Analysis Date = 09/23/14 Pct Recovery = 27% Analysis Date = 09/23/14 Pct Recovery = 27% Analysis Date = 09/18/14 Pct Recovery = 27% Analysis Date = 09/18/14 Pct Recovery = 27% Analysis Date = 09/13/14 Pct Recovery = 27% Analysis Date = 09/13/14 Pct Recovery = 27% Analysis Date = 09/09/14 Pct Recovery = 26% Analysis Date = 09/09/14 Pct Recovery = 26% Analysis Date = 09/04/14 Pct Recovery = 26% Analysis Date = 09/04/14 Pct Recovery = 26% Analysis Date = 08/31/14 Pct Recovery = 25% Analysis Date = 08/31/14 Pct Recovery = 25% Analysis Date = 08/26/14 Pct Recovery = 25% Analysis Date = 08/26/14 Pct Recovery = 25% Analysis Date = 08/22/14 Pct Recovery = 25% Analysis Date = 08/22/14 Pct Recovery = 25% Analysis Date = 08/17/14 Pct Recovery = 24% Analysis Date = 08/17/14 Pct Recovery = 24% Analysis Date = 08/13/14 Pct Recovery = 24% Analysis Date = 08/13/14 Pct Recovery = 24% Analysis Date = 08/08/14 Pct Recovery = 23% Analysis Date = 08/08/14 Pct Recovery = 23% Analysis Date = 08/04/14 Pct Recovery = 23% Analysis Date = 08/04/14 Pct Recovery = 23% Analysis Date = 07/30/14 Pct Recovery = 23% Analysis Date = 07/30/14 Pct Recovery = 23% Analysis Date = 07/26/14 Pct Recovery = 22% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
TIOTROPIUM

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 3 33% 2% 32% 4%
>= Reporting Level 41 33% 27% 28% 24%
Total 44 33% 26% 30% 23%

Sample Statistics
TIOTROPIUM

Characteristic N % % Basis
Plotted 44 85% Spiked
Estimated Values 44 85% Spiked
Deleted Values 1 1% Spiked + Not Spiked
Spiked, Censored 2 4% Spiked
Spiked 52 .  
False Negatives 6 12% 6 out of 52
Not Spiked 63 .  
False Positives 0 0% 0 out of 62

BQS OBSP Determination:
TRAMADOL
METHOD: 2440 , TESTIDCODE: 67517LCM56
Open Data Set

Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 84% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 82% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 80 µl & ERA 0406-15-08: 80 µl Pct Recovery = 83% Analysis Date = 11/04/15 SpikeMix = Abs 052215: 80 µl & Abs 050115: 80 µl Pct Recovery = 90% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 80% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 83% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 93% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 94% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-04: 15 µl & Abs 041814: 15 µl Pct Recovery = 71% Analysis Date = 12/06/14 SpikeMix = ERA 0318-14-02: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 72% Analysis Date = 10/25/14 SpikeMix = Abs 041614: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 76% Analysis Date = 10/11/14 SpikeMix = ERA 0318-14-02: 60 µl & ERA 0319-14-04: 60 µl Pct Recovery = 66% Analysis Date = 08/28/14 SpikeMix = ERA 0319-14-04: 60 µl & ERA 0319-14-05: 60 µl Pct Recovery = 57% Analysis Date = 05/07/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 92% Analysis Date = 03/11/15 SpikeMix = ERA 0318-14-02: 15 µl & Abs 041714: 15 µl Pct Recovery = 90% Analysis Date = 01/16/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 86% Analysis Date = 12/06/14 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 72% Analysis Date = 08/21/14 SpikeMix = ERA 0318-14-02: 60 µl & Abs 041714: 60 µl Pct Recovery = 71% Analysis Date = 07/12/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 77% Analysis Date = 06/11/14 SpikeMix = Abs 041614: 60 µl & Abs 041714: 60 µl Pct Recovery = 81% Analysis Date = 05/21/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 98% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 81% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 68% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 76% Analysis Date = 02/23/16 SpikeMix = Abs 052215: 40 µl & Abs 050115: 40 µl Pct Recovery = 86% Analysis Date = 07/31/15 SpikeMix = ERA 0406-15-09: 40 µl & Abs 050115: 40 µl Pct Recovery = 90% Analysis Date = 07/30/15 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 90% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 80% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 79% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 77% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 78% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 66% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 66% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 67% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 63% Analysis Date = 04/30/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 81% Analysis Date = 04/10/15 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 69% Analysis Date = 02/10/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 76% Analysis Date = 12/07/14 SpikeMix = ERA 0318-14-02: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 78% Analysis Date = 10/11/14 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 59% Analysis Date = 11/04/14 SpikeMix = Abs 041714: 8 µl & ERA 0319-14-05: 8 µl Pct Recovery = 75% Analysis Date = 09/12/14 SpikeMix = Abs 041614: 30 µl & ERA 0319-14-04: 30 µl Pct Recovery = 56% Analysis Date = 08/16/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 60% Analysis Date = 07/13/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 66% Analysis Date = 10/10/14 SpikeMix = Abs 041714: 30 µl & Abs 041814: 30 µl Pct Recovery = 69% Analysis Date = 07/20/14 SpikeMix = ERA 0318-14-02: 30 µl & Abs 041714: 30 µl Pct Recovery = 64% Analysis Date = 06/28/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 80% Analysis Date = 05/17/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 87% Analysis Date = 11/25/15 SpikeMix = Abs 050115: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 83% Analysis Date = 11/24/15 SpikeMix = ERA 0406-15-09: 20 µl & Abs 050115: 20 µl Pct Recovery = 90% Analysis Date = 08/27/15 SpikeMix = Abs 052215: 20 µl & Abs 050115: 20 µl Pct Recovery = 81% Analysis Date = 08/11/15 SpikeMix = Abs 050115: 20 µl & Abs 051315: 20 µl Pct Recovery = 57% Analysis Date = 07/09/15 SpikeMix = Abs 050115: 20 µl & Abs 052215: 20 µl Pct Recovery = 71% Analysis Date = 06/09/15 SpikeMix = Abs 051315: 20 µl & Abs 050115: 20 µl Pct Recovery = 66% Analysis Date = 01/18/17 Pct Recovery = 78% Analysis Date = 01/14/17 Pct Recovery = 78% Analysis Date = 01/14/17 Pct Recovery = 78% Analysis Date = 01/09/17 Pct Recovery = 78% Analysis Date = 01/09/17 Pct Recovery = 78% Analysis Date = 01/04/17 Pct Recovery = 78% Analysis Date = 01/04/17 Pct Recovery = 78% Analysis Date = 12/30/16 Pct Recovery = 78% Analysis Date = 12/30/16 Pct Recovery = 78% Analysis Date = 12/25/16 Pct Recovery = 78% Analysis Date = 12/25/16 Pct Recovery = 78% Analysis Date = 12/20/16 Pct Recovery = 78% Analysis Date = 12/20/16 Pct Recovery = 78% Analysis Date = 12/15/16 Pct Recovery = 78% Analysis Date = 12/15/16 Pct Recovery = 78% Analysis Date = 12/10/16 Pct Recovery = 78% Analysis Date = 12/10/16 Pct Recovery = 78% Analysis Date = 12/05/16 Pct Recovery = 78% Analysis Date = 12/05/16 Pct Recovery = 78% Analysis Date = 12/01/16 Pct Recovery = 78% Analysis Date = 12/01/16 Pct Recovery = 78% Analysis Date = 11/26/16 Pct Recovery = 78% Analysis Date = 11/26/16 Pct Recovery = 78% Analysis Date = 11/21/16 Pct Recovery = 78% Analysis Date = 11/21/16 Pct Recovery = 78% Analysis Date = 11/16/16 Pct Recovery = 78% Analysis Date = 11/16/16 Pct Recovery = 78% Analysis Date = 11/11/16 Pct Recovery = 78% Analysis Date = 11/11/16 Pct Recovery = 78% Analysis Date = 11/06/16 Pct Recovery = 78% Analysis Date = 11/06/16 Pct Recovery = 78% Analysis Date = 11/01/16 Pct Recovery = 78% Analysis Date = 11/01/16 Pct Recovery = 78% Analysis Date = 10/27/16 Pct Recovery = 78% Analysis Date = 10/27/16 Pct Recovery = 78% Analysis Date = 10/22/16 Pct Recovery = 78% Analysis Date = 10/22/16 Pct Recovery = 78% Analysis Date = 10/18/16 Pct Recovery = 78% Analysis Date = 10/18/16 Pct Recovery = 78% Analysis Date = 10/13/16 Pct Recovery = 78% Analysis Date = 10/13/16 Pct Recovery = 78% Analysis Date = 10/08/16 Pct Recovery = 78% Analysis Date = 10/08/16 Pct Recovery = 78% Analysis Date = 10/03/16 Pct Recovery = 78% Analysis Date = 10/03/16 Pct Recovery = 78% Analysis Date = 09/28/16 Pct Recovery = 78% Analysis Date = 09/28/16 Pct Recovery = 78% Analysis Date = 09/23/16 Pct Recovery = 78% Analysis Date = 09/23/16 Pct Recovery = 78% Analysis Date = 09/18/16 Pct Recovery = 78% Analysis Date = 09/18/16 Pct Recovery = 78% Analysis Date = 09/13/16 Pct Recovery = 78% Analysis Date = 09/13/16 Pct Recovery = 78% Analysis Date = 09/08/16 Pct Recovery = 78% Analysis Date = 09/08/16 Pct Recovery = 78% Analysis Date = 09/04/16 Pct Recovery = 78% Analysis Date = 09/04/16 Pct Recovery = 78% Analysis Date = 08/30/16 Pct Recovery = 78% Analysis Date = 08/30/16 Pct Recovery = 78% Analysis Date = 08/25/16 Pct Recovery = 78% Analysis Date = 08/25/16 Pct Recovery = 78% Analysis Date = 08/20/16 Pct Recovery = 78% Analysis Date = 08/20/16 Pct Recovery = 78% Analysis Date = 08/15/16 Pct Recovery = 78% Analysis Date = 08/15/16 Pct Recovery = 78% Analysis Date = 08/10/16 Pct Recovery = 79% Analysis Date = 08/10/16 Pct Recovery = 79% Analysis Date = 08/05/16 Pct Recovery = 79% Analysis Date = 08/05/16 Pct Recovery = 79% Analysis Date = 07/31/16 Pct Recovery = 79% Analysis Date = 07/31/16 Pct Recovery = 79% Analysis Date = 07/26/16 Pct Recovery = 79% Analysis Date = 07/26/16 Pct Recovery = 79% Analysis Date = 07/22/16 Pct Recovery = 79% Analysis Date = 07/22/16 Pct Recovery = 79% Analysis Date = 07/17/16 Pct Recovery = 79% Analysis Date = 07/17/16 Pct Recovery = 79% Analysis Date = 07/12/16 Pct Recovery = 79% Analysis Date = 07/12/16 Pct Recovery = 79% Analysis Date = 07/07/16 Pct Recovery = 79% Analysis Date = 07/07/16 Pct Recovery = 79% Analysis Date = 07/02/16 Pct Recovery = 79% Analysis Date = 07/02/16 Pct Recovery = 79% Analysis Date = 06/27/16 Pct Recovery = 79% Analysis Date = 06/27/16 Pct Recovery = 79% Analysis Date = 06/22/16 Pct Recovery = 79% Analysis Date = 06/22/16 Pct Recovery = 79% Analysis Date = 06/17/16 Pct Recovery = 79% Analysis Date = 06/17/16 Pct Recovery = 79% Analysis Date = 06/12/16 Pct Recovery = 79% Analysis Date = 06/12/16 Pct Recovery = 79% Analysis Date = 06/08/16 Pct Recovery = 79% Analysis Date = 06/08/16 Pct Recovery = 79% Analysis Date = 06/03/16 Pct Recovery = 79% Analysis Date = 06/03/16 Pct Recovery = 79% Analysis Date = 05/29/16 Pct Recovery = 79% Analysis Date = 05/29/16 Pct Recovery = 79% Analysis Date = 05/24/16 Pct Recovery = 79% Analysis Date = 05/24/16 Pct Recovery = 79% Analysis Date = 05/19/16 Pct Recovery = 79% Analysis Date = 05/19/16 Pct Recovery = 79% Analysis Date = 05/14/16 Pct Recovery = 79% Analysis Date = 05/14/16 Pct Recovery = 79% Analysis Date = 05/09/16 Pct Recovery = 79% Analysis Date = 05/09/16 Pct Recovery = 79% Analysis Date = 05/04/16 Pct Recovery = 79% Analysis Date = 05/04/16 Pct Recovery = 79% Analysis Date = 04/29/16 Pct Recovery = 79% Analysis Date = 04/29/16 Pct Recovery = 79% Analysis Date = 04/25/16 Pct Recovery = 79% Analysis Date = 04/25/16 Pct Recovery = 79% Analysis Date = 04/20/16 Pct Recovery = 79% Analysis Date = 04/20/16 Pct Recovery = 79% Analysis Date = 04/15/16 Pct Recovery = 79% Analysis Date = 04/15/16 Pct Recovery = 79% Analysis Date = 04/10/16 Pct Recovery = 79% Analysis Date = 04/10/16 Pct Recovery = 79% Analysis Date = 04/05/16 Pct Recovery = 79% Analysis Date = 04/05/16 Pct Recovery = 79% Analysis Date = 03/31/16 Pct Recovery = 79% Analysis Date = 03/31/16 Pct Recovery = 79% Analysis Date = 03/26/16 Pct Recovery = 79% Analysis Date = 03/26/16 Pct Recovery = 79% Analysis Date = 03/21/16 Pct Recovery = 80% Analysis Date = 03/21/16 Pct Recovery = 80% Analysis Date = 03/16/16 Pct Recovery = 80% Analysis Date = 03/16/16 Pct Recovery = 80% Analysis Date = 03/12/16 Pct Recovery = 80% Analysis Date = 03/12/16 Pct Recovery = 80% Analysis Date = 03/07/16 Pct Recovery = 80% Analysis Date = 03/07/16 Pct Recovery = 80% Analysis Date = 03/02/16 Pct Recovery = 80% Analysis Date = 03/02/16 Pct Recovery = 80% Analysis Date = 02/26/16 Pct Recovery = 80% Analysis Date = 02/26/16 Pct Recovery = 80% Analysis Date = 02/21/16 Pct Recovery = 80% Analysis Date = 02/21/16 Pct Recovery = 80% Analysis Date = 02/16/16 Pct Recovery = 80% Analysis Date = 02/16/16 Pct Recovery = 80% Analysis Date = 02/11/16 Pct Recovery = 80% Analysis Date = 02/11/16 Pct Recovery = 80% Analysis Date = 02/06/16 Pct Recovery = 80% Analysis Date = 02/06/16 Pct Recovery = 80% Analysis Date = 02/01/16 Pct Recovery = 80% Analysis Date = 02/01/16 Pct Recovery = 80% Analysis Date = 01/28/16 Pct Recovery = 80% Analysis Date = 01/28/16 Pct Recovery = 80% Analysis Date = 01/23/16 Pct Recovery = 80% Analysis Date = 01/23/16 Pct Recovery = 80% Analysis Date = 01/18/16 Pct Recovery = 80% Analysis Date = 01/18/16 Pct Recovery = 80% Analysis Date = 01/13/16 Pct Recovery = 80% Analysis Date = 01/13/16 Pct Recovery = 80% Analysis Date = 01/08/16 Pct Recovery = 80% Analysis Date = 01/08/16 Pct Recovery = 80% Analysis Date = 01/03/16 Pct Recovery = 80% Analysis Date = 01/03/16 Pct Recovery = 80% Analysis Date = 12/29/15 Pct Recovery = 80% Analysis Date = 12/29/15 Pct Recovery = 80% Analysis Date = 12/24/15 Pct Recovery = 80% Analysis Date = 12/24/15 Pct Recovery = 80% Analysis Date = 12/19/15 Pct Recovery = 80% Analysis Date = 12/19/15 Pct Recovery = 80% Analysis Date = 12/15/15 Pct Recovery = 80% Analysis Date = 12/15/15 Pct Recovery = 80% Analysis Date = 12/10/15 Pct Recovery = 80% Analysis Date = 12/10/15 Pct Recovery = 80% Analysis Date = 12/05/15 Pct Recovery = 80% Analysis Date = 12/05/15 Pct Recovery = 80% Analysis Date = 11/30/15 Pct Recovery = 80% Analysis Date = 11/30/15 Pct Recovery = 80% Analysis Date = 11/25/15 Pct Recovery = 80% Analysis Date = 11/25/15 Pct Recovery = 80% Analysis Date = 11/20/15 Pct Recovery = 80% Analysis Date = 11/20/15 Pct Recovery = 80% Analysis Date = 11/15/15 Pct Recovery = 80% Analysis Date = 11/15/15 Pct Recovery = 80% Analysis Date = 11/10/15 Pct Recovery = 80% Analysis Date = 11/10/15 Pct Recovery = 80% Analysis Date = 11/05/15 Pct Recovery = 80% Analysis Date = 11/05/15 Pct Recovery = 80% Analysis Date = 11/01/15 Pct Recovery = 80% Analysis Date = 11/01/15 Pct Recovery = 80% Analysis Date = 10/27/15 Pct Recovery = 80% Analysis Date = 10/27/15 Pct Recovery = 80% Analysis Date = 10/22/15 Pct Recovery = 80% Analysis Date = 10/22/15 Pct Recovery = 80% Analysis Date = 10/17/15 Pct Recovery = 80% Analysis Date = 10/17/15 Pct Recovery = 80% Analysis Date = 10/12/15 Pct Recovery = 80% Analysis Date = 10/12/15 Pct Recovery = 80% Analysis Date = 10/07/15 Pct Recovery = 80% Analysis Date = 10/07/15 Pct Recovery = 80% Analysis Date = 10/02/15 Pct Recovery = 80% Analysis Date = 10/02/15 Pct Recovery = 80% Analysis Date = 09/27/15 Pct Recovery = 80% Analysis Date = 09/27/15 Pct Recovery = 80% Analysis Date = 09/22/15 Pct Recovery = 80% Analysis Date = 09/22/15 Pct Recovery = 80% Analysis Date = 09/17/15 Pct Recovery = 80% Analysis Date = 09/17/15 Pct Recovery = 80% Analysis Date = 09/13/15 Pct Recovery = 80% Analysis Date = 09/13/15 Pct Recovery = 80% Analysis Date = 09/08/15 Pct Recovery = 80% Analysis Date = 09/08/15 Pct Recovery = 80% Analysis Date = 09/03/15 Pct Recovery = 80% Analysis Date = 09/03/15 Pct Recovery = 80% Analysis Date = 08/29/15 Pct Recovery = 80% Analysis Date = 08/29/15 Pct Recovery = 80% Analysis Date = 08/24/15 Pct Recovery = 80% Analysis Date = 08/24/15 Pct Recovery = 80% Analysis Date = 08/19/15 Pct Recovery = 80% Analysis Date = 08/19/15 Pct Recovery = 80% Analysis Date = 08/14/15 Pct Recovery = 80% Analysis Date = 08/14/15 Pct Recovery = 80% Analysis Date = 08/09/15 Pct Recovery = 80% Analysis Date = 08/09/15 Pct Recovery = 80% Analysis Date = 08/04/15 Pct Recovery = 80% Analysis Date = 08/04/15 Pct Recovery = 80% Analysis Date = 07/31/15 Pct Recovery = 80% Analysis Date = 07/31/15 Pct Recovery = 80% Analysis Date = 07/26/15 Pct Recovery = 80% Analysis Date = 07/26/15 Pct Recovery = 80% Analysis Date = 07/21/15 Pct Recovery = 80% Analysis Date = 07/21/15 Pct Recovery = 80% Analysis Date = 07/16/15 Pct Recovery = 80% Analysis Date = 07/16/15 Pct Recovery = 80% Analysis Date = 07/11/15 Pct Recovery = 80% Analysis Date = 07/11/15 Pct Recovery = 80% Analysis Date = 07/06/15 Pct Recovery = 79% Analysis Date = 07/06/15 Pct Recovery = 79% Analysis Date = 07/01/15 Pct Recovery = 79% Analysis Date = 07/01/15 Pct Recovery = 79% Analysis Date = 06/26/15 Pct Recovery = 79% Analysis Date = 06/26/15 Pct Recovery = 79% Analysis Date = 06/21/15 Pct Recovery = 79% Analysis Date = 06/21/15 Pct Recovery = 79% Analysis Date = 06/17/15 Pct Recovery = 79% Analysis Date = 06/17/15 Pct Recovery = 79% Analysis Date = 06/12/15 Pct Recovery = 79% Analysis Date = 06/12/15 Pct Recovery = 79% Analysis Date = 06/07/15 Pct Recovery = 79% Analysis Date = 06/07/15 Pct Recovery = 79% Analysis Date = 06/02/15 Pct Recovery = 79% Analysis Date = 06/02/15 Pct Recovery = 79% Analysis Date = 05/28/15 Pct Recovery = 79% Analysis Date = 05/28/15 Pct Recovery = 79% Analysis Date = 05/23/15 Pct Recovery = 78% Analysis Date = 05/23/15 Pct Recovery = 78% Analysis Date = 05/18/15 Pct Recovery = 78% Analysis Date = 05/18/15 Pct Recovery = 78% Analysis Date = 05/13/15 Pct Recovery = 78% Analysis Date = 05/13/15 Pct Recovery = 78% Analysis Date = 05/08/15 Pct Recovery = 78% Analysis Date = 05/08/15 Pct Recovery = 78% Analysis Date = 05/04/15 Pct Recovery = 78% Analysis Date = 05/04/15 Pct Recovery = 78% Analysis Date = 04/29/15 Pct Recovery = 78% Analysis Date = 04/29/15 Pct Recovery = 78% Analysis Date = 04/24/15 Pct Recovery = 77% Analysis Date = 04/24/15 Pct Recovery = 77% Analysis Date = 04/19/15 Pct Recovery = 77% Analysis Date = 04/19/15 Pct Recovery = 77% Analysis Date = 04/14/15 Pct Recovery = 77% Analysis Date = 04/14/15 Pct Recovery = 77% Analysis Date = 04/09/15 Pct Recovery = 77% Analysis Date = 04/09/15 Pct Recovery = 77% Analysis Date = 04/04/15 Pct Recovery = 77% Analysis Date = 04/04/15 Pct Recovery = 77% Analysis Date = 03/30/15 Pct Recovery = 77% Analysis Date = 03/30/15 Pct Recovery = 77% Analysis Date = 03/25/15 Pct Recovery = 76% Analysis Date = 03/25/15 Pct Recovery = 76% Analysis Date = 03/21/15 Pct Recovery = 76% Analysis Date = 03/21/15 Pct Recovery = 76% Analysis Date = 03/16/15 Pct Recovery = 76% Analysis Date = 03/16/15 Pct Recovery = 76% Analysis Date = 03/11/15 Pct Recovery = 76% Analysis Date = 03/11/15 Pct Recovery = 76% Analysis Date = 03/06/15 Pct Recovery = 76% Analysis Date = 03/06/15 Pct Recovery = 76% Analysis Date = 03/01/15 Pct Recovery = 76% Analysis Date = 03/01/15 Pct Recovery = 76% Analysis Date = 02/24/15 Pct Recovery = 75% Analysis Date = 02/24/15 Pct Recovery = 75% Analysis Date = 02/19/15 Pct Recovery = 75% Analysis Date = 02/19/15 Pct Recovery = 75% Analysis Date = 02/14/15 Pct Recovery = 75% Analysis Date = 02/14/15 Pct Recovery = 75% Analysis Date = 02/09/15 Pct Recovery = 75% Analysis Date = 02/09/15 Pct Recovery = 75% Analysis Date = 02/05/15 Pct Recovery = 75% Analysis Date = 02/05/15 Pct Recovery = 75% Analysis Date = 01/31/15 Pct Recovery = 75% Analysis Date = 01/31/15 Pct Recovery = 75% Analysis Date = 01/26/15 Pct Recovery = 75% Analysis Date = 01/26/15 Pct Recovery = 75% Analysis Date = 01/21/15 Pct Recovery = 74% Analysis Date = 01/21/15 Pct Recovery = 74% Analysis Date = 01/16/15 Pct Recovery = 74% Analysis Date = 01/16/15 Pct Recovery = 74% Analysis Date = 01/11/15 Pct Recovery = 74% Analysis Date = 01/11/15 Pct Recovery = 74% Analysis Date = 01/06/15 Pct Recovery = 74% Analysis Date = 01/06/15 Pct Recovery = 74% Analysis Date = 01/01/15 Pct Recovery = 74% Analysis Date = 01/01/15 Pct Recovery = 74% Analysis Date = 12/27/14 Pct Recovery = 74% Analysis Date = 12/27/14 Pct Recovery = 74% Analysis Date = 12/23/14 Pct Recovery = 74% Analysis Date = 12/23/14 Pct Recovery = 74% Analysis Date = 12/18/14 Pct Recovery = 74% Analysis Date = 12/18/14 Pct Recovery = 74% Analysis Date = 12/13/14 Pct Recovery = 73% Analysis Date = 12/13/14 Pct Recovery = 73% Analysis Date = 12/08/14 Pct Recovery = 73% Analysis Date = 12/08/14 Pct Recovery = 73% Analysis Date = 12/03/14 Pct Recovery = 73% Analysis Date = 12/03/14 Pct Recovery = 73% Analysis Date = 11/28/14 Pct Recovery = 73% Analysis Date = 11/28/14 Pct Recovery = 73% Analysis Date = 11/23/14 Pct Recovery = 73% Analysis Date = 11/23/14 Pct Recovery = 73% Analysis Date = 11/18/14 Pct Recovery = 73% Analysis Date = 11/18/14 Pct Recovery = 73% Analysis Date = 11/13/14 Pct Recovery = 73% Analysis Date = 11/13/14 Pct Recovery = 73% Analysis Date = 11/09/14 Pct Recovery = 73% Analysis Date = 11/09/14 Pct Recovery = 73% Analysis Date = 11/04/14 Pct Recovery = 73% Analysis Date = 11/04/14 Pct Recovery = 73% Analysis Date = 10/30/14 Pct Recovery = 73% Analysis Date = 10/30/14 Pct Recovery = 73% Analysis Date = 10/25/14 Pct Recovery = 73% Analysis Date = 10/25/14 Pct Recovery = 73% Analysis Date = 10/20/14 Pct Recovery = 73% Analysis Date = 10/20/14 Pct Recovery = 73% Analysis Date = 10/15/14 Pct Recovery = 73% Analysis Date = 10/15/14 Pct Recovery = 73% Analysis Date = 10/10/14 Pct Recovery = 73% Analysis Date = 10/10/14 Pct Recovery = 73% Analysis Date = 10/05/14 Pct Recovery = 73% Analysis Date = 10/05/14 Pct Recovery = 73% Analysis Date = 09/30/14 Pct Recovery = 73% Analysis Date = 09/30/14 Pct Recovery = 73% Analysis Date = 09/26/14 Pct Recovery = 73% Analysis Date = 09/26/14 Pct Recovery = 73% Analysis Date = 09/21/14 Pct Recovery = 73% Analysis Date = 09/21/14 Pct Recovery = 73% Analysis Date = 09/16/14 Pct Recovery = 73% Analysis Date = 09/16/14 Pct Recovery = 73% Analysis Date = 09/11/14 Pct Recovery = 73% Analysis Date = 09/11/14 Pct Recovery = 73% Analysis Date = 09/06/14 Pct Recovery = 73% Analysis Date = 09/06/14 Pct Recovery = 73% Analysis Date = 09/01/14 Pct Recovery = 73% Analysis Date = 09/01/14 Pct Recovery = 73% Analysis Date = 08/27/14 Pct Recovery = 73% Analysis Date = 08/27/14 Pct Recovery = 73% Analysis Date = 08/22/14 Pct Recovery = 73% Analysis Date = 08/22/14 Pct Recovery = 73% Analysis Date = 08/17/14 Pct Recovery = 73% Analysis Date = 08/17/14 Pct Recovery = 73% Analysis Date = 08/13/14 Pct Recovery = 73% Analysis Date = 08/13/14 Pct Recovery = 73% Analysis Date = 08/08/14 Pct Recovery = 73% Analysis Date = 08/08/14 Pct Recovery = 73% Analysis Date = 08/03/14 Pct Recovery = 73% Analysis Date = 08/03/14 Pct Recovery = 73% Analysis Date = 07/29/14 Pct Recovery = 73% Analysis Date = 07/29/14 Pct Recovery = 73% Analysis Date = 07/24/14 Pct Recovery = 73% Analysis Date = 07/24/14 Pct Recovery = 73% Analysis Date = 07/19/14 Pct Recovery = 73% Analysis Date = 07/19/14 Pct Recovery = 73% Analysis Date = 07/14/14 Pct Recovery = 73% Analysis Date = 07/14/14 Pct Recovery = 73% Analysis Date = 07/09/14 Pct Recovery = 73% Analysis Date = 07/09/14 Pct Recovery = 73% Analysis Date = 07/04/14 Pct Recovery = 73% Analysis Date = 07/04/14 Pct Recovery = 73% Analysis Date = 06/30/14 Pct Recovery = 73% Analysis Date = 06/30/14 Pct Recovery = 73% Analysis Date = 06/25/14 Pct Recovery = 73% Analysis Date = 06/25/14 Pct Recovery = 73% Analysis Date = 06/20/14 Pct Recovery = 74% Analysis Date = 06/20/14 Pct Recovery = 74% Analysis Date = 06/15/14 Pct Recovery = 74% Analysis Date = 06/15/14 Pct Recovery = 74% Analysis Date = 06/10/14 Pct Recovery = 74% Analysis Date = 06/10/14 Pct Recovery = 74% Analysis Date = 06/05/14 Pct Recovery = 74% Analysis Date = 06/05/14 Pct Recovery = 74% Analysis Date = 05/31/14 Pct Recovery = 74% Analysis Date = 05/31/14 Pct Recovery = 74% Analysis Date = 05/26/14 Pct Recovery = 74% Analysis Date = 05/26/14 Pct Recovery = 74% Analysis Date = 05/21/14 Pct Recovery = 74% Analysis Date = 05/21/14 Pct Recovery = 74% Analysis Date = 05/17/14 Pct Recovery = 74% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
TRAMADOL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 54 77% 11% 78% 11%
Total 54 77% 11% 78% 11%

Sample Statistics
TRAMADOL

Characteristic N % % Basis
Plotted 54 100% Spiked
Estimated Values 4 7% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 54 .  
False Negatives 0 0% 0 out of 54
Not Spiked 61 .  
False Positives 0 0% 0 out of 61

BQS OBSP Determination:
TRIAMTERENE
METHOD: 2440 , TESTIDCODE: 67475LCM56
Open Data Set

Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 80% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 75% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 81% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 82% Analysis Date = 01/17/16 SpikeMix = ERA 0406-15-09: 80 µl & ERA 0406-15-07A: 80 µl Pct Recovery = 72% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 80 µl & Abs 051315: 80 µl Pct Recovery = 65% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 80 µl & ERA 0406-15-08: 80 µl Pct Recovery = 86% Analysis Date = 11/04/15 SpikeMix = Abs 052215: 80 µl & Abs 050115: 80 µl Pct Recovery = 83% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 72% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 70% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 85% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 77% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 73% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 77% Analysis Date = 09/24/16 SpikeMix = Crescent EN160610015: 80 µl & Abs 061416: 80 µl Pct Recovery = 79% Analysis Date = 09/24/16 SpikeMix = Abs 061416: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 71% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-04: 15 µl & Abs 041814: 15 µl Pct Recovery = 76% Analysis Date = 02/06/15 SpikeMix = Abs 041814: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 78% Analysis Date = 07/12/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 87% Analysis Date = 06/22/14 SpikeMix = Abs 041814: 60 µl & Abs 041614: 60 µl Pct Recovery = 94% Analysis Date = 05/21/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 125% Analysis Date = 05/07/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 106% Analysis Date = 04/29/15 SpikeMix = ERA 0319-14-05: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 86% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 80% Analysis Date = 01/16/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 84% Analysis Date = 12/07/14 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 82% Analysis Date = 12/06/14 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 68% Analysis Date = 08/28/14 SpikeMix = ERA 0319-14-04: 60 µl & ERA 0319-14-05: 60 µl Pct Recovery = 64% Analysis Date = 07/26/14 SpikeMix = ERA 0319-14-05: 60 µl & ERA 0318-14-02: 60 µl Pct Recovery = 106% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-07A: 40 µl & Abs 051315: 40 µl Pct Recovery = 55% Analysis Date = 11/04/15 SpikeMix = ERA 0406-15-07A: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 56% Analysis Date = 09/10/15 SpikeMix = Abs 052215: 40 µl & ERA 0406-15-07A: 40 µl Pct Recovery = 60% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 76% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 66% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 83% Analysis Date = 02/23/16 SpikeMix = Abs 052215: 40 µl & Abs 050115: 40 µl Pct Recovery = 85% Analysis Date = 07/31/15 SpikeMix = ERA 0406-15-09: 40 µl & Abs 050115: 40 µl Pct Recovery = 80% Analysis Date = 07/30/15 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 83% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 68% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 70% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 66% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 66% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 53% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 55% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 63% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 48% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 61% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 66% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 72% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 72% Analysis Date = 04/10/15 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 68% Analysis Date = 11/04/14 SpikeMix = Abs 041814: 8 µl & ERA 0318-14-02: 8 µl Pct Recovery = 60% Analysis Date = 10/11/14 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 47% Analysis Date = 11/04/14 SpikeMix = Abs 041714: 8 µl & ERA 0319-14-05: 8 µl Pct Recovery = 73% Analysis Date = 10/24/14 SpikeMix = ERA 0319-14-05: 8 µl & Abs 041614: 8 µl Pct Recovery = 75% Analysis Date = 10/10/14 SpikeMix = Abs 041714: 30 µl & Abs 041814: 30 µl Pct Recovery = 59% Analysis Date = 10/10/14 SpikeMix = Abs 041814: 30 µl & ERA 0318-14-02: 30 µl Pct Recovery = 62% Analysis Date = 07/13/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 81% Analysis Date = 05/30/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 107% Analysis Date = 08/30/14 SpikeMix = ERA 0318-14-02: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 90% Analysis Date = 08/16/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 53% Analysis Date = 07/13/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 96% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 59% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 51% Analysis Date = 04/27/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 88% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 79% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 79% Analysis Date = 11/24/15 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 67% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-09: 20 µl Pct Recovery = 56% Analysis Date = 09/15/15 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 81% Analysis Date = 11/25/15 SpikeMix = Abs 050115: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 84% Analysis Date = 11/24/15 SpikeMix = ERA 0406-15-09: 20 µl & Abs 050115: 20 µl Pct Recovery = 76% Analysis Date = 08/27/15 SpikeMix = Abs 052215: 20 µl & Abs 050115: 20 µl Pct Recovery = 69% Analysis Date = 08/11/15 SpikeMix = Abs 050115: 20 µl & Abs 051315: 20 µl Pct Recovery = 64% Analysis Date = 07/09/15 SpikeMix = Abs 050115: 20 µl & Abs 052215: 20 µl Pct Recovery = 63% Analysis Date = 06/09/15 SpikeMix = Abs 051315: 20 µl & Abs 050115: 20 µl Pct Recovery = 90% Analysis Date = 01/18/17 Pct Recovery = 71% Analysis Date = 01/14/17 Pct Recovery = 71% Analysis Date = 01/14/17 Pct Recovery = 71% Analysis Date = 01/09/17 Pct Recovery = 71% Analysis Date = 01/09/17 Pct Recovery = 71% Analysis Date = 01/04/17 Pct Recovery = 71% Analysis Date = 01/04/17 Pct Recovery = 71% Analysis Date = 12/30/16 Pct Recovery = 71% Analysis Date = 12/30/16 Pct Recovery = 71% Analysis Date = 12/25/16 Pct Recovery = 71% Analysis Date = 12/25/16 Pct Recovery = 71% Analysis Date = 12/20/16 Pct Recovery = 71% Analysis Date = 12/20/16 Pct Recovery = 71% Analysis Date = 12/15/16 Pct Recovery = 71% Analysis Date = 12/15/16 Pct Recovery = 71% Analysis Date = 12/11/16 Pct Recovery = 71% Analysis Date = 12/11/16 Pct Recovery = 71% Analysis Date = 12/06/16 Pct Recovery = 71% Analysis Date = 12/06/16 Pct Recovery = 71% Analysis Date = 12/01/16 Pct Recovery = 71% Analysis Date = 12/01/16 Pct Recovery = 71% Analysis Date = 11/26/16 Pct Recovery = 71% Analysis Date = 11/26/16 Pct Recovery = 71% Analysis Date = 11/21/16 Pct Recovery = 71% Analysis Date = 11/21/16 Pct Recovery = 71% Analysis Date = 11/16/16 Pct Recovery = 71% Analysis Date = 11/16/16 Pct Recovery = 71% Analysis Date = 11/11/16 Pct Recovery = 71% Analysis Date = 11/11/16 Pct Recovery = 71% Analysis Date = 11/06/16 Pct Recovery = 71% Analysis Date = 11/06/16 Pct Recovery = 71% Analysis Date = 11/02/16 Pct Recovery = 71% Analysis Date = 11/02/16 Pct Recovery = 71% Analysis Date = 10/28/16 Pct Recovery = 71% Analysis Date = 10/28/16 Pct Recovery = 71% Analysis Date = 10/23/16 Pct Recovery = 71% Analysis Date = 10/23/16 Pct Recovery = 71% Analysis Date = 10/18/16 Pct Recovery = 71% Analysis Date = 10/18/16 Pct Recovery = 71% Analysis Date = 10/13/16 Pct Recovery = 71% Analysis Date = 10/13/16 Pct Recovery = 71% Analysis Date = 10/08/16 Pct Recovery = 71% Analysis Date = 10/08/16 Pct Recovery = 71% Analysis Date = 10/03/16 Pct Recovery = 71% Analysis Date = 10/03/16 Pct Recovery = 71% Analysis Date = 09/28/16 Pct Recovery = 71% Analysis Date = 09/28/16 Pct Recovery = 71% Analysis Date = 09/24/16 Pct Recovery = 71% Analysis Date = 09/24/16 Pct Recovery = 71% Analysis Date = 09/19/16 Pct Recovery = 71% Analysis Date = 09/19/16 Pct Recovery = 71% Analysis Date = 09/14/16 Pct Recovery = 71% Analysis Date = 09/14/16 Pct Recovery = 71% Analysis Date = 09/09/16 Pct Recovery = 71% Analysis Date = 09/09/16 Pct Recovery = 71% Analysis Date = 09/04/16 Pct Recovery = 71% Analysis Date = 09/04/16 Pct Recovery = 71% Analysis Date = 08/30/16 Pct Recovery = 71% Analysis Date = 08/30/16 Pct Recovery = 71% Analysis Date = 08/25/16 Pct Recovery = 71% Analysis Date = 08/25/16 Pct Recovery = 71% Analysis Date = 08/21/16 Pct Recovery = 71% Analysis Date = 08/21/16 Pct Recovery = 71% Analysis Date = 08/16/16 Pct Recovery = 71% Analysis Date = 08/16/16 Pct Recovery = 71% Analysis Date = 08/11/16 Pct Recovery = 71% Analysis Date = 08/11/16 Pct Recovery = 71% Analysis Date = 08/06/16 Pct Recovery = 71% Analysis Date = 08/06/16 Pct Recovery = 71% Analysis Date = 08/01/16 Pct Recovery = 71% Analysis Date = 08/01/16 Pct Recovery = 71% Analysis Date = 07/27/16 Pct Recovery = 71% Analysis Date = 07/27/16 Pct Recovery = 71% Analysis Date = 07/22/16 Pct Recovery = 71% Analysis Date = 07/22/16 Pct Recovery = 71% Analysis Date = 07/17/16 Pct Recovery = 71% Analysis Date = 07/17/16 Pct Recovery = 71% Analysis Date = 07/13/16 Pct Recovery = 71% Analysis Date = 07/13/16 Pct Recovery = 71% Analysis Date = 07/08/16 Pct Recovery = 71% Analysis Date = 07/08/16 Pct Recovery = 71% Analysis Date = 07/03/16 Pct Recovery = 71% Analysis Date = 07/03/16 Pct Recovery = 71% Analysis Date = 06/28/16 Pct Recovery = 71% Analysis Date = 06/28/16 Pct Recovery = 71% Analysis Date = 06/23/16 Pct Recovery = 71% Analysis Date = 06/23/16 Pct Recovery = 71% Analysis Date = 06/18/16 Pct Recovery = 71% Analysis Date = 06/18/16 Pct Recovery = 71% Analysis Date = 06/13/16 Pct Recovery = 71% Analysis Date = 06/13/16 Pct Recovery = 71% Analysis Date = 06/08/16 Pct Recovery = 71% Analysis Date = 06/08/16 Pct Recovery = 71% Analysis Date = 06/04/16 Pct Recovery = 71% Analysis Date = 06/04/16 Pct Recovery = 71% Analysis Date = 05/30/16 Pct Recovery = 72% Analysis Date = 05/30/16 Pct Recovery = 72% Analysis Date = 05/25/16 Pct Recovery = 72% Analysis Date = 05/25/16 Pct Recovery = 72% Analysis Date = 05/20/16 Pct Recovery = 72% Analysis Date = 05/20/16 Pct Recovery = 72% Analysis Date = 05/15/16 Pct Recovery = 72% Analysis Date = 05/15/16 Pct Recovery = 72% Analysis Date = 05/10/16 Pct Recovery = 72% Analysis Date = 05/10/16 Pct Recovery = 72% Analysis Date = 05/05/16 Pct Recovery = 72% Analysis Date = 05/05/16 Pct Recovery = 72% Analysis Date = 05/01/16 Pct Recovery = 72% Analysis Date = 05/01/16 Pct Recovery = 72% Analysis Date = 04/26/16 Pct Recovery = 72% Analysis Date = 04/26/16 Pct Recovery = 72% Analysis Date = 04/21/16 Pct Recovery = 72% Analysis Date = 04/21/16 Pct Recovery = 72% Analysis Date = 04/16/16 Pct Recovery = 72% Analysis Date = 04/16/16 Pct Recovery = 72% Analysis Date = 04/11/16 Pct Recovery = 72% Analysis Date = 04/11/16 Pct Recovery = 72% Analysis Date = 04/06/16 Pct Recovery = 72% Analysis Date = 04/06/16 Pct Recovery = 72% Analysis Date = 04/01/16 Pct Recovery = 72% Analysis Date = 04/01/16 Pct Recovery = 72% Analysis Date = 03/27/16 Pct Recovery = 72% Analysis Date = 03/27/16 Pct Recovery = 72% Analysis Date = 03/23/16 Pct Recovery = 72% Analysis Date = 03/23/16 Pct Recovery = 72% Analysis Date = 03/18/16 Pct Recovery = 72% Analysis Date = 03/18/16 Pct Recovery = 72% Analysis Date = 03/13/16 Pct Recovery = 72% Analysis Date = 03/13/16 Pct Recovery = 72% Analysis Date = 03/08/16 Pct Recovery = 72% Analysis Date = 03/08/16 Pct Recovery = 72% Analysis Date = 03/03/16 Pct Recovery = 72% Analysis Date = 03/03/16 Pct Recovery = 72% Analysis Date = 02/27/16 Pct Recovery = 72% Analysis Date = 02/27/16 Pct Recovery = 72% Analysis Date = 02/22/16 Pct Recovery = 72% Analysis Date = 02/22/16 Pct Recovery = 72% Analysis Date = 02/17/16 Pct Recovery = 72% Analysis Date = 02/17/16 Pct Recovery = 72% Analysis Date = 02/13/16 Pct Recovery = 72% Analysis Date = 02/13/16 Pct Recovery = 72% Analysis Date = 02/08/16 Pct Recovery = 72% Analysis Date = 02/08/16 Pct Recovery = 72% Analysis Date = 02/03/16 Pct Recovery = 72% Analysis Date = 02/03/16 Pct Recovery = 72% Analysis Date = 01/29/16 Pct Recovery = 72% Analysis Date = 01/29/16 Pct Recovery = 72% Analysis Date = 01/24/16 Pct Recovery = 72% Analysis Date = 01/24/16 Pct Recovery = 72% Analysis Date = 01/19/16 Pct Recovery = 72% Analysis Date = 01/19/16 Pct Recovery = 72% Analysis Date = 01/14/16 Pct Recovery = 72% Analysis Date = 01/14/16 Pct Recovery = 72% Analysis Date = 01/10/16 Pct Recovery = 72% Analysis Date = 01/10/16 Pct Recovery = 72% Analysis Date = 01/05/16 Pct Recovery = 73% Analysis Date = 01/05/16 Pct Recovery = 73% Analysis Date = 12/31/15 Pct Recovery = 73% Analysis Date = 12/31/15 Pct Recovery = 73% Analysis Date = 12/26/15 Pct Recovery = 73% Analysis Date = 12/26/15 Pct Recovery = 73% Analysis Date = 12/21/15 Pct Recovery = 73% Analysis Date = 12/21/15 Pct Recovery = 73% Analysis Date = 12/16/15 Pct Recovery = 73% Analysis Date = 12/16/15 Pct Recovery = 73% Analysis Date = 12/11/15 Pct Recovery = 73% Analysis Date = 12/11/15 Pct Recovery = 73% Analysis Date = 12/06/15 Pct Recovery = 73% Analysis Date = 12/06/15 Pct Recovery = 73% Analysis Date = 12/02/15 Pct Recovery = 73% Analysis Date = 12/02/15 Pct Recovery = 73% Analysis Date = 11/27/15 Pct Recovery = 73% Analysis Date = 11/27/15 Pct Recovery = 73% Analysis Date = 11/22/15 Pct Recovery = 73% Analysis Date = 11/22/15 Pct Recovery = 73% Analysis Date = 11/17/15 Pct Recovery = 73% Analysis Date = 11/17/15 Pct Recovery = 73% Analysis Date = 11/12/15 Pct Recovery = 73% Analysis Date = 11/12/15 Pct Recovery = 73% Analysis Date = 11/07/15 Pct Recovery = 73% Analysis Date = 11/07/15 Pct Recovery = 73% Analysis Date = 11/02/15 Pct Recovery = 73% Analysis Date = 11/02/15 Pct Recovery = 73% Analysis Date = 10/28/15 Pct Recovery = 74% Analysis Date = 10/28/15 Pct Recovery = 74% Analysis Date = 10/24/15 Pct Recovery = 74% Analysis Date = 10/24/15 Pct Recovery = 74% Analysis Date = 10/19/15 Pct Recovery = 74% Analysis Date = 10/19/15 Pct Recovery = 74% Analysis Date = 10/14/15 Pct Recovery = 74% Analysis Date = 10/14/15 Pct Recovery = 74% Analysis Date = 10/09/15 Pct Recovery = 74% Analysis Date = 10/09/15 Pct Recovery = 74% Analysis Date = 10/04/15 Pct Recovery = 74% Analysis Date = 10/04/15 Pct Recovery = 74% Analysis Date = 09/29/15 Pct Recovery = 74% Analysis Date = 09/29/15 Pct Recovery = 74% Analysis Date = 09/24/15 Pct Recovery = 74% Analysis Date = 09/24/15 Pct Recovery = 74% Analysis Date = 09/19/15 Pct Recovery = 74% Analysis Date = 09/19/15 Pct Recovery = 74% Analysis Date = 09/15/15 Pct Recovery = 74% Analysis Date = 09/15/15 Pct Recovery = 74% Analysis Date = 09/10/15 Pct Recovery = 74% Analysis Date = 09/10/15 Pct Recovery = 74% Analysis Date = 09/05/15 Pct Recovery = 74% Analysis Date = 09/05/15 Pct Recovery = 74% Analysis Date = 08/31/15 Pct Recovery = 74% Analysis Date = 08/31/15 Pct Recovery = 74% Analysis Date = 08/26/15 Pct Recovery = 74% Analysis Date = 08/26/15 Pct Recovery = 74% Analysis Date = 08/21/15 Pct Recovery = 75% Analysis Date = 08/21/15 Pct Recovery = 75% Analysis Date = 08/16/15 Pct Recovery = 75% Analysis Date = 08/16/15 Pct Recovery = 75% Analysis Date = 08/12/15 Pct Recovery = 75% Analysis Date = 08/12/15 Pct Recovery = 75% Analysis Date = 08/07/15 Pct Recovery = 75% Analysis Date = 08/07/15 Pct Recovery = 75% Analysis Date = 08/02/15 Pct Recovery = 75% Analysis Date = 08/02/15 Pct Recovery = 75% Analysis Date = 07/28/15 Pct Recovery = 75% Analysis Date = 07/28/15 Pct Recovery = 75% Analysis Date = 07/23/15 Pct Recovery = 75% Analysis Date = 07/23/15 Pct Recovery = 75% Analysis Date = 07/18/15 Pct Recovery = 75% Analysis Date = 07/18/15 Pct Recovery = 75% Analysis Date = 07/13/15 Pct Recovery = 75% Analysis Date = 07/13/15 Pct Recovery = 75% Analysis Date = 07/08/15 Pct Recovery = 75% Analysis Date = 07/08/15 Pct Recovery = 75% Analysis Date = 07/04/15 Pct Recovery = 75% Analysis Date = 07/04/15 Pct Recovery = 75% Analysis Date = 06/29/15 Pct Recovery = 75% Analysis Date = 06/29/15 Pct Recovery = 75% Analysis Date = 06/24/15 Pct Recovery = 75% Analysis Date = 06/24/15 Pct Recovery = 75% Analysis Date = 06/19/15 Pct Recovery = 75% Analysis Date = 06/19/15 Pct Recovery = 75% Analysis Date = 06/14/15 Pct Recovery = 75% Analysis Date = 06/14/15 Pct Recovery = 75% Analysis Date = 06/09/15 Pct Recovery = 74% Analysis Date = 06/09/15 Pct Recovery = 74% Analysis Date = 06/04/15 Pct Recovery = 74% Analysis Date = 06/04/15 Pct Recovery = 74% Analysis Date = 05/30/15 Pct Recovery = 74% Analysis Date = 05/30/15 Pct Recovery = 74% Analysis Date = 05/26/15 Pct Recovery = 74% Analysis Date = 05/26/15 Pct Recovery = 74% Analysis Date = 05/21/15 Pct Recovery = 74% Analysis Date = 05/21/15 Pct Recovery = 74% Analysis Date = 05/16/15 Pct Recovery = 74% Analysis Date = 05/16/15 Pct Recovery = 74% Analysis Date = 05/11/15 Pct Recovery = 74% Analysis Date = 05/11/15 Pct Recovery = 74% Analysis Date = 05/06/15 Pct Recovery = 74% Analysis Date = 05/06/15 Pct Recovery = 74% Analysis Date = 05/01/15 Pct Recovery = 74% Analysis Date = 05/01/15 Pct Recovery = 74% Analysis Date = 04/26/15 Pct Recovery = 74% Analysis Date = 04/26/15 Pct Recovery = 74% Analysis Date = 04/22/15 Pct Recovery = 74% Analysis Date = 04/22/15 Pct Recovery = 74% Analysis Date = 04/17/15 Pct Recovery = 74% Analysis Date = 04/17/15 Pct Recovery = 74% Analysis Date = 04/12/15 Pct Recovery = 75% Analysis Date = 04/12/15 Pct Recovery = 75% Analysis Date = 04/07/15 Pct Recovery = 75% Analysis Date = 04/07/15 Pct Recovery = 75% Analysis Date = 04/02/15 Pct Recovery = 75% Analysis Date = 04/02/15 Pct Recovery = 75% Analysis Date = 03/28/15 Pct Recovery = 75% Analysis Date = 03/28/15 Pct Recovery = 75% Analysis Date = 03/23/15 Pct Recovery = 75% Analysis Date = 03/23/15 Pct Recovery = 75% Analysis Date = 03/18/15 Pct Recovery = 75% Analysis Date = 03/18/15 Pct Recovery = 75% Analysis Date = 03/14/15 Pct Recovery = 75% Analysis Date = 03/14/15 Pct Recovery = 75% Analysis Date = 03/09/15 Pct Recovery = 76% Analysis Date = 03/09/15 Pct Recovery = 76% Analysis Date = 03/04/15 Pct Recovery = 76% Analysis Date = 03/04/15 Pct Recovery = 76% Analysis Date = 02/27/15 Pct Recovery = 76% Analysis Date = 02/27/15 Pct Recovery = 76% Analysis Date = 02/22/15 Pct Recovery = 76% Analysis Date = 02/22/15 Pct Recovery = 76% Analysis Date = 02/17/15 Pct Recovery = 76% Analysis Date = 02/17/15 Pct Recovery = 76% Analysis Date = 02/12/15 Pct Recovery = 76% Analysis Date = 02/12/15 Pct Recovery = 76% Analysis Date = 02/07/15 Pct Recovery = 76% Analysis Date = 02/07/15 Pct Recovery = 76% Analysis Date = 02/03/15 Pct Recovery = 76% Analysis Date = 02/03/15 Pct Recovery = 76% Analysis Date = 01/29/15 Pct Recovery = 77% Analysis Date = 01/29/15 Pct Recovery = 77% Analysis Date = 01/24/15 Pct Recovery = 77% Analysis Date = 01/24/15 Pct Recovery = 77% Analysis Date = 01/19/15 Pct Recovery = 77% Analysis Date = 01/19/15 Pct Recovery = 77% Analysis Date = 01/14/15 Pct Recovery = 77% Analysis Date = 01/14/15 Pct Recovery = 77% Analysis Date = 01/09/15 Pct Recovery = 77% Analysis Date = 01/09/15 Pct Recovery = 77% Analysis Date = 01/04/15 Pct Recovery = 77% Analysis Date = 01/04/15 Pct Recovery = 77% Analysis Date = 12/31/14 Pct Recovery = 78% Analysis Date = 12/31/14 Pct Recovery = 78% Analysis Date = 12/26/14 Pct Recovery = 78% Analysis Date = 12/26/14 Pct Recovery = 78% Analysis Date = 12/21/14 Pct Recovery = 78% Analysis Date = 12/21/14 Pct Recovery = 78% Analysis Date = 12/16/14 Pct Recovery = 78% Analysis Date = 12/16/14 Pct Recovery = 78% Analysis Date = 12/11/14 Pct Recovery = 78% Analysis Date = 12/11/14 Pct Recovery = 78% Analysis Date = 12/06/14 Pct Recovery = 79% Analysis Date = 12/06/14 Pct Recovery = 79% Analysis Date = 12/01/14 Pct Recovery = 79% Analysis Date = 12/01/14 Pct Recovery = 79% Analysis Date = 11/26/14 Pct Recovery = 79% Analysis Date = 11/26/14 Pct Recovery = 79% Analysis Date = 11/22/14 Pct Recovery = 79% Analysis Date = 11/22/14 Pct Recovery = 79% Analysis Date = 11/17/14 Pct Recovery = 79% Analysis Date = 11/17/14 Pct Recovery = 79% Analysis Date = 11/12/14 Pct Recovery = 80% Analysis Date = 11/12/14 Pct Recovery = 80% Analysis Date = 11/07/14 Pct Recovery = 80% Analysis Date = 11/07/14 Pct Recovery = 80% Analysis Date = 11/02/14 Pct Recovery = 80% Analysis Date = 11/02/14 Pct Recovery = 80% Analysis Date = 10/28/14 Pct Recovery = 80% Analysis Date = 10/28/14 Pct Recovery = 80% Analysis Date = 10/23/14 Pct Recovery = 80% Analysis Date = 10/23/14 Pct Recovery = 80% Analysis Date = 10/18/14 Pct Recovery = 80% Analysis Date = 10/18/14 Pct Recovery = 80% Analysis Date = 10/14/14 Pct Recovery = 81% Analysis Date = 10/14/14 Pct Recovery = 81% Analysis Date = 10/09/14 Pct Recovery = 81% Analysis Date = 10/09/14 Pct Recovery = 81% Analysis Date = 10/04/14 Pct Recovery = 81% Analysis Date = 10/04/14 Pct Recovery = 81% Analysis Date = 09/29/14 Pct Recovery = 81% Analysis Date = 09/29/14 Pct Recovery = 81% Analysis Date = 09/24/14 Pct Recovery = 81% Analysis Date = 09/24/14 Pct Recovery = 81% Analysis Date = 09/19/14 Pct Recovery = 82% Analysis Date = 09/19/14 Pct Recovery = 82% Analysis Date = 09/14/14 Pct Recovery = 82% Analysis Date = 09/14/14 Pct Recovery = 82% Analysis Date = 09/10/14 Pct Recovery = 82% Analysis Date = 09/10/14 Pct Recovery = 82% Analysis Date = 09/05/14 Pct Recovery = 82% Analysis Date = 09/05/14 Pct Recovery = 82% Analysis Date = 08/31/14 Pct Recovery = 82% Analysis Date = 08/31/14 Pct Recovery = 82% Analysis Date = 08/26/14 Pct Recovery = 83% Analysis Date = 08/26/14 Pct Recovery = 83% Analysis Date = 08/21/14 Pct Recovery = 83% Analysis Date = 08/21/14 Pct Recovery = 83% Analysis Date = 08/16/14 Pct Recovery = 83% Analysis Date = 08/16/14 Pct Recovery = 83% Analysis Date = 08/11/14 Pct Recovery = 83% Analysis Date = 08/11/14 Pct Recovery = 83% Analysis Date = 08/06/14 Pct Recovery = 83% Analysis Date = 08/06/14 Pct Recovery = 83% Analysis Date = 08/02/14 Pct Recovery = 84% Analysis Date = 08/02/14 Pct Recovery = 84% Analysis Date = 07/28/14 Pct Recovery = 84% Analysis Date = 07/28/14 Pct Recovery = 84% Analysis Date = 07/23/14 Pct Recovery = 84% Analysis Date = 07/23/14 Pct Recovery = 84% Analysis Date = 07/18/14 Pct Recovery = 84% Analysis Date = 07/18/14 Pct Recovery = 84% Analysis Date = 07/13/14 Pct Recovery = 84% Analysis Date = 07/13/14 Pct Recovery = 84% Analysis Date = 07/08/14 Pct Recovery = 85% Analysis Date = 07/08/14 Pct Recovery = 85% Analysis Date = 07/03/14 Pct Recovery = 85% Analysis Date = 07/03/14 Pct Recovery = 85% Analysis Date = 06/28/14 Pct Recovery = 85% Analysis Date = 06/28/14 Pct Recovery = 85% Analysis Date = 06/24/14 Pct Recovery = 85% Analysis Date = 06/24/14 Pct Recovery = 85% Analysis Date = 06/19/14 Pct Recovery = 85% Analysis Date = 06/19/14 Pct Recovery = 85% Analysis Date = 06/14/14 Pct Recovery = 86% Analysis Date = 06/14/14 Pct Recovery = 86% Analysis Date = 06/09/14 Pct Recovery = 86% Analysis Date = 06/09/14 Pct Recovery = 86% Analysis Date = 06/04/14 Pct Recovery = 86% Analysis Date = 06/04/14 Pct Recovery = 86% Analysis Date = 05/30/14 Pct Recovery = 86% Analysis Date = 05/30/14 Pct Recovery = 86% Analysis Date = 05/25/14 Pct Recovery = 86% Analysis Date = 05/25/14 Pct Recovery = 86% Analysis Date = 05/21/14 Pct Recovery = 87% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
TRIAMTERENE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 76 74% 14% 74% 13%
Total 76 74% 14% 74% 13%

Sample Statistics
TRIAMTERENE

Characteristic N % % Basis
Plotted 76 99% Spiked
Estimated Values 14 18% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 77 .  
False Negatives 1 1% 1 out of 77
Not Spiked 38 .  
False Positives 0 0% 0 out of 38

BQS OBSP Determination:
TRIMETHOPRIM
METHOD: 2440 , TESTIDCODE: 67456LCM56
Open Data Set

Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 88% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 85% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 86% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 99% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 80 µl & ERA 0406-15-08: 80 µl Pct Recovery = 78% Analysis Date = 11/04/15 SpikeMix = Abs 052215: 80 µl & Abs 050115: 80 µl Pct Recovery = 87% Analysis Date = 01/17/16 SpikeMix = ERA 0406-15-09: 80 µl & ERA 0406-15-07A: 80 µl Pct Recovery = 62% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 80 µl & Abs 051315: 80 µl Pct Recovery = 41% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 74% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 83% Analysis Date = 09/24/16 SpikeMix = Crescent EN160610015: 80 µl & Abs 061416: 80 µl Pct Recovery = 67% Analysis Date = 09/24/16 SpikeMix = Abs 061416: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 66% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 82% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 80% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 79% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 84% Analysis Date = 04/29/15 SpikeMix = ERA 0319-14-05: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 133% Analysis Date = 03/11/15 SpikeMix = ERA 0318-14-02: 15 µl & Abs 041714: 15 µl Pct Recovery = 108% Analysis Date = 02/06/15 SpikeMix = Abs 041814: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 91% Analysis Date = 12/06/14 SpikeMix = ERA 0318-14-02: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 98% Analysis Date = 10/11/14 SpikeMix = ERA 0318-14-02: 60 µl & ERA 0319-14-04: 60 µl Pct Recovery = 98% Analysis Date = 08/21/14 SpikeMix = ERA 0318-14-02: 60 µl & Abs 041714: 60 µl Pct Recovery = 100% Analysis Date = 07/26/14 SpikeMix = ERA 0319-14-05: 60 µl & ERA 0318-14-02: 60 µl Pct Recovery = 109% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 103% Analysis Date = 12/07/14 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 94% Analysis Date = 10/25/14 SpikeMix = Abs 041614: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 96% Analysis Date = 06/22/14 SpikeMix = Abs 041814: 60 µl & Abs 041614: 60 µl Pct Recovery = 90% Analysis Date = 06/11/14 SpikeMix = Abs 041614: 60 µl & Abs 041714: 60 µl Pct Recovery = 127% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 79% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 65% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 74% Analysis Date = 02/23/16 SpikeMix = Abs 052215: 40 µl & Abs 050115: 40 µl Pct Recovery = 85% Analysis Date = 07/31/15 SpikeMix = ERA 0406-15-09: 40 µl & Abs 050115: 40 µl Pct Recovery = 86% Analysis Date = 07/30/15 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 76% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-07A: 40 µl & Abs 051315: 40 µl Pct Recovery = 44% Analysis Date = 11/04/15 SpikeMix = ERA 0406-15-07A: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 53% Analysis Date = 09/10/15 SpikeMix = Abs 052215: 40 µl & ERA 0406-15-07A: 40 µl Pct Recovery = 57% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 69% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 66% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 70% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 70% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 81% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 77% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 83% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 70% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 77% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 80% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 74% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 65% Analysis Date = 12/07/14 SpikeMix = ERA 0318-14-02: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 105% Analysis Date = 11/04/14 SpikeMix = Abs 041814: 8 µl & ERA 0318-14-02: 8 µl Pct Recovery = 107% Analysis Date = 04/30/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 120% Analysis Date = 02/10/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 84% Analysis Date = 10/24/14 SpikeMix = ERA 0319-14-05: 8 µl & Abs 041614: 8 µl Pct Recovery = 99% Analysis Date = 10/10/14 SpikeMix = Abs 041814: 30 µl & ERA 0318-14-02: 30 µl Pct Recovery = 108% Analysis Date = 08/30/14 SpikeMix = ERA 0318-14-02: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 111% Analysis Date = 07/20/14 SpikeMix = ERA 0318-14-02: 30 µl & Abs 041714: 30 µl Pct Recovery = 45% Analysis Date = 09/12/14 SpikeMix = Abs 041614: 30 µl & ERA 0319-14-04: 30 µl Pct Recovery = 60% Analysis Date = 07/13/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 64% Analysis Date = 06/28/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 95% Analysis Date = 05/30/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 93% Analysis Date = 05/17/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 121% Analysis Date = 11/25/15 SpikeMix = Abs 050115: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 70% Analysis Date = 11/24/15 SpikeMix = ERA 0406-15-09: 20 µl & Abs 050115: 20 µl Pct Recovery = 88% Analysis Date = 08/27/15 SpikeMix = Abs 052215: 20 µl & Abs 050115: 20 µl Pct Recovery = 87% Analysis Date = 08/11/15 SpikeMix = Abs 050115: 20 µl & Abs 051315: 20 µl Pct Recovery = 54% Analysis Date = 07/09/15 SpikeMix = Abs 050115: 20 µl & Abs 052215: 20 µl Pct Recovery = 92% Analysis Date = 06/09/15 SpikeMix = Abs 051315: 20 µl & Abs 050115: 20 µl Pct Recovery = 75% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 58% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 45% Analysis Date = 04/27/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 72% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 43% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 50% Analysis Date = 11/24/15 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 59% Analysis Date = 09/15/15 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 52% Analysis Date = 01/18/17 Pct Recovery = 83% Analysis Date = 01/14/17 Pct Recovery = 82% Analysis Date = 01/14/17 Pct Recovery = 82% Analysis Date = 01/09/17 Pct Recovery = 82% Analysis Date = 01/09/17 Pct Recovery = 82% Analysis Date = 01/04/17 Pct Recovery = 82% Analysis Date = 01/04/17 Pct Recovery = 82% Analysis Date = 12/30/16 Pct Recovery = 82% Analysis Date = 12/30/16 Pct Recovery = 82% Analysis Date = 12/25/16 Pct Recovery = 81% Analysis Date = 12/25/16 Pct Recovery = 81% Analysis Date = 12/20/16 Pct Recovery = 81% Analysis Date = 12/20/16 Pct Recovery = 81% Analysis Date = 12/15/16 Pct Recovery = 81% Analysis Date = 12/15/16 Pct Recovery = 81% Analysis Date = 12/10/16 Pct Recovery = 80% Analysis Date = 12/10/16 Pct Recovery = 80% Analysis Date = 12/05/16 Pct Recovery = 80% Analysis Date = 12/05/16 Pct Recovery = 80% Analysis Date = 12/01/16 Pct Recovery = 80% Analysis Date = 12/01/16 Pct Recovery = 80% Analysis Date = 11/26/16 Pct Recovery = 79% Analysis Date = 11/26/16 Pct Recovery = 79% Analysis Date = 11/21/16 Pct Recovery = 79% Analysis Date = 11/21/16 Pct Recovery = 79% Analysis Date = 11/16/16 Pct Recovery = 79% Analysis Date = 11/16/16 Pct Recovery = 79% Analysis Date = 11/11/16 Pct Recovery = 79% Analysis Date = 11/11/16 Pct Recovery = 79% Analysis Date = 11/06/16 Pct Recovery = 78% Analysis Date = 11/06/16 Pct Recovery = 78% Analysis Date = 11/01/16 Pct Recovery = 78% Analysis Date = 11/01/16 Pct Recovery = 78% Analysis Date = 10/27/16 Pct Recovery = 78% Analysis Date = 10/27/16 Pct Recovery = 78% Analysis Date = 10/22/16 Pct Recovery = 77% Analysis Date = 10/22/16 Pct Recovery = 77% Analysis Date = 10/18/16 Pct Recovery = 77% Analysis Date = 10/18/16 Pct Recovery = 77% Analysis Date = 10/13/16 Pct Recovery = 77% Analysis Date = 10/13/16 Pct Recovery = 77% Analysis Date = 10/08/16 Pct Recovery = 77% Analysis Date = 10/08/16 Pct Recovery = 77% Analysis Date = 10/03/16 Pct Recovery = 76% Analysis Date = 10/03/16 Pct Recovery = 76% Analysis Date = 09/28/16 Pct Recovery = 76% Analysis Date = 09/28/16 Pct Recovery = 76% Analysis Date = 09/23/16 Pct Recovery = 76% Analysis Date = 09/23/16 Pct Recovery = 76% Analysis Date = 09/18/16 Pct Recovery = 76% Analysis Date = 09/18/16 Pct Recovery = 76% Analysis Date = 09/13/16 Pct Recovery = 75% Analysis Date = 09/13/16 Pct Recovery = 75% Analysis Date = 09/08/16 Pct Recovery = 75% Analysis Date = 09/08/16 Pct Recovery = 75% Analysis Date = 09/04/16 Pct Recovery = 75% Analysis Date = 09/04/16 Pct Recovery = 75% Analysis Date = 08/30/16 Pct Recovery = 74% Analysis Date = 08/30/16 Pct Recovery = 74% Analysis Date = 08/25/16 Pct Recovery = 74% Analysis Date = 08/25/16 Pct Recovery = 74% Analysis Date = 08/20/16 Pct Recovery = 74% Analysis Date = 08/20/16 Pct Recovery = 74% Analysis Date = 08/15/16 Pct Recovery = 74% Analysis Date = 08/15/16 Pct Recovery = 74% Analysis Date = 08/10/16 Pct Recovery = 73% Analysis Date = 08/10/16 Pct Recovery = 73% Analysis Date = 08/05/16 Pct Recovery = 73% Analysis Date = 08/05/16 Pct Recovery = 73% Analysis Date = 07/31/16 Pct Recovery = 73% Analysis Date = 07/31/16 Pct Recovery = 73% Analysis Date = 07/26/16 Pct Recovery = 73% Analysis Date = 07/26/16 Pct Recovery = 73% Analysis Date = 07/22/16 Pct Recovery = 73% Analysis Date = 07/22/16 Pct Recovery = 73% Analysis Date = 07/17/16 Pct Recovery = 72% Analysis Date = 07/17/16 Pct Recovery = 72% Analysis Date = 07/12/16 Pct Recovery = 72% Analysis Date = 07/12/16 Pct Recovery = 72% Analysis Date = 07/07/16 Pct Recovery = 72% Analysis Date = 07/07/16 Pct Recovery = 72% Analysis Date = 07/02/16 Pct Recovery = 72% Analysis Date = 07/02/16 Pct Recovery = 72% Analysis Date = 06/27/16 Pct Recovery = 71% Analysis Date = 06/27/16 Pct Recovery = 71% Analysis Date = 06/22/16 Pct Recovery = 71% Analysis Date = 06/22/16 Pct Recovery = 71% Analysis Date = 06/17/16 Pct Recovery = 71% Analysis Date = 06/17/16 Pct Recovery = 71% Analysis Date = 06/12/16 Pct Recovery = 71% Analysis Date = 06/12/16 Pct Recovery = 71% Analysis Date = 06/08/16 Pct Recovery = 71% Analysis Date = 06/08/16 Pct Recovery = 71% Analysis Date = 06/03/16 Pct Recovery = 70% Analysis Date = 06/03/16 Pct Recovery = 70% Analysis Date = 05/29/16 Pct Recovery = 70% Analysis Date = 05/29/16 Pct Recovery = 70% Analysis Date = 05/24/16 Pct Recovery = 70% Analysis Date = 05/24/16 Pct Recovery = 70% Analysis Date = 05/19/16 Pct Recovery = 70% Analysis Date = 05/19/16 Pct Recovery = 70% Analysis Date = 05/14/16 Pct Recovery = 69% Analysis Date = 05/14/16 Pct Recovery = 69% Analysis Date = 05/09/16 Pct Recovery = 69% Analysis Date = 05/09/16 Pct Recovery = 69% Analysis Date = 05/04/16 Pct Recovery = 69% Analysis Date = 05/04/16 Pct Recovery = 69% Analysis Date = 04/29/16 Pct Recovery = 69% Analysis Date = 04/29/16 Pct Recovery = 69% Analysis Date = 04/25/16 Pct Recovery = 69% Analysis Date = 04/25/16 Pct Recovery = 69% Analysis Date = 04/20/16 Pct Recovery = 68% Analysis Date = 04/20/16 Pct Recovery = 68% Analysis Date = 04/15/16 Pct Recovery = 68% Analysis Date = 04/15/16 Pct Recovery = 68% Analysis Date = 04/10/16 Pct Recovery = 68% Analysis Date = 04/10/16 Pct Recovery = 68% Analysis Date = 04/05/16 Pct Recovery = 68% Analysis Date = 04/05/16 Pct Recovery = 68% Analysis Date = 03/31/16 Pct Recovery = 68% Analysis Date = 03/31/16 Pct Recovery = 68% Analysis Date = 03/26/16 Pct Recovery = 68% Analysis Date = 03/26/16 Pct Recovery = 68% Analysis Date = 03/21/16 Pct Recovery = 68% Analysis Date = 03/21/16 Pct Recovery = 68% Analysis Date = 03/16/16 Pct Recovery = 67% Analysis Date = 03/16/16 Pct Recovery = 67% Analysis Date = 03/12/16 Pct Recovery = 67% Analysis Date = 03/12/16 Pct Recovery = 67% Analysis Date = 03/07/16 Pct Recovery = 67% Analysis Date = 03/07/16 Pct Recovery = 67% Analysis Date = 03/02/16 Pct Recovery = 67% Analysis Date = 03/02/16 Pct Recovery = 67% Analysis Date = 02/26/16 Pct Recovery = 67% Analysis Date = 02/26/16 Pct Recovery = 67% Analysis Date = 02/21/16 Pct Recovery = 67% Analysis Date = 02/21/16 Pct Recovery = 67% Analysis Date = 02/16/16 Pct Recovery = 67% Analysis Date = 02/16/16 Pct Recovery = 67% Analysis Date = 02/11/16 Pct Recovery = 67% Analysis Date = 02/11/16 Pct Recovery = 67% Analysis Date = 02/06/16 Pct Recovery = 67% Analysis Date = 02/06/16 Pct Recovery = 67% Analysis Date = 02/01/16 Pct Recovery = 67% Analysis Date = 02/01/16 Pct Recovery = 67% Analysis Date = 01/28/16 Pct Recovery = 67% Analysis Date = 01/28/16 Pct Recovery = 67% Analysis Date = 01/23/16 Pct Recovery = 68% Analysis Date = 01/23/16 Pct Recovery = 68% Analysis Date = 01/18/16 Pct Recovery = 68% Analysis Date = 01/18/16 Pct Recovery = 68% Analysis Date = 01/13/16 Pct Recovery = 68% Analysis Date = 01/13/16 Pct Recovery = 68% Analysis Date = 01/08/16 Pct Recovery = 68% Analysis Date = 01/08/16 Pct Recovery = 68% Analysis Date = 01/03/16 Pct Recovery = 68% Analysis Date = 01/03/16 Pct Recovery = 68% Analysis Date = 12/29/15 Pct Recovery = 68% Analysis Date = 12/29/15 Pct Recovery = 68% Analysis Date = 12/24/15 Pct Recovery = 68% Analysis Date = 12/24/15 Pct Recovery = 68% Analysis Date = 12/19/15 Pct Recovery = 68% Analysis Date = 12/19/15 Pct Recovery = 68% Analysis Date = 12/15/15 Pct Recovery = 69% Analysis Date = 12/15/15 Pct Recovery = 69% Analysis Date = 12/10/15 Pct Recovery = 69% Analysis Date = 12/10/15 Pct Recovery = 69% Analysis Date = 12/05/15 Pct Recovery = 69% Analysis Date = 12/05/15 Pct Recovery = 69% Analysis Date = 11/30/15 Pct Recovery = 69% Analysis Date = 11/30/15 Pct Recovery = 69% Analysis Date = 11/25/15 Pct Recovery = 69% Analysis Date = 11/25/15 Pct Recovery = 69% Analysis Date = 11/20/15 Pct Recovery = 70% Analysis Date = 11/20/15 Pct Recovery = 70% Analysis Date = 11/15/15 Pct Recovery = 70% Analysis Date = 11/15/15 Pct Recovery = 70% Analysis Date = 11/10/15 Pct Recovery = 70% Analysis Date = 11/10/15 Pct Recovery = 70% Analysis Date = 11/05/15 Pct Recovery = 71% Analysis Date = 11/05/15 Pct Recovery = 71% Analysis Date = 11/01/15 Pct Recovery = 71% Analysis Date = 11/01/15 Pct Recovery = 71% Analysis Date = 10/27/15 Pct Recovery = 72% Analysis Date = 10/27/15 Pct Recovery = 72% Analysis Date = 10/22/15 Pct Recovery = 72% Analysis Date = 10/22/15 Pct Recovery = 72% Analysis Date = 10/17/15 Pct Recovery = 73% Analysis Date = 10/17/15 Pct Recovery = 73% Analysis Date = 10/12/15 Pct Recovery = 73% Analysis Date = 10/12/15 Pct Recovery = 73% Analysis Date = 10/07/15 Pct Recovery = 74% Analysis Date = 10/07/15 Pct Recovery = 74% Analysis Date = 10/02/15 Pct Recovery = 74% Analysis Date = 10/02/15 Pct Recovery = 74% Analysis Date = 09/27/15 Pct Recovery = 75% Analysis Date = 09/27/15 Pct Recovery = 75% Analysis Date = 09/22/15 Pct Recovery = 75% Analysis Date = 09/22/15 Pct Recovery = 75% Analysis Date = 09/17/15 Pct Recovery = 76% Analysis Date = 09/17/15 Pct Recovery = 76% Analysis Date = 09/13/15 Pct Recovery = 76% Analysis Date = 09/13/15 Pct Recovery = 76% Analysis Date = 09/08/15 Pct Recovery = 76% Analysis Date = 09/08/15 Pct Recovery = 76% Analysis Date = 09/03/15 Pct Recovery = 77% Analysis Date = 09/03/15 Pct Recovery = 77% Analysis Date = 08/29/15 Pct Recovery = 77% Analysis Date = 08/29/15 Pct Recovery = 77% Analysis Date = 08/24/15 Pct Recovery = 78% Analysis Date = 08/24/15 Pct Recovery = 78% Analysis Date = 08/19/15 Pct Recovery = 78% Analysis Date = 08/19/15 Pct Recovery = 78% Analysis Date = 08/14/15 Pct Recovery = 79% Analysis Date = 08/14/15 Pct Recovery = 79% Analysis Date = 08/09/15 Pct Recovery = 79% Analysis Date = 08/09/15 Pct Recovery = 79% Analysis Date = 08/04/15 Pct Recovery = 80% Analysis Date = 08/04/15 Pct Recovery = 80% Analysis Date = 07/31/15 Pct Recovery = 80% Analysis Date = 07/31/15 Pct Recovery = 80% Analysis Date = 07/26/15 Pct Recovery = 81% Analysis Date = 07/26/15 Pct Recovery = 81% Analysis Date = 07/21/15 Pct Recovery = 81% Analysis Date = 07/21/15 Pct Recovery = 81% Analysis Date = 07/16/15 Pct Recovery = 81% Analysis Date = 07/16/15 Pct Recovery = 81% Analysis Date = 07/11/15 Pct Recovery = 82% Analysis Date = 07/11/15 Pct Recovery = 82% Analysis Date = 07/06/15 Pct Recovery = 82% Analysis Date = 07/06/15 Pct Recovery = 82% Analysis Date = 07/01/15 Pct Recovery = 82% Analysis Date = 07/01/15 Pct Recovery = 82% Analysis Date = 06/26/15 Pct Recovery = 83% Analysis Date = 06/26/15 Pct Recovery = 83% Analysis Date = 06/21/15 Pct Recovery = 83% Analysis Date = 06/21/15 Pct Recovery = 83% Analysis Date = 06/17/15 Pct Recovery = 83% Analysis Date = 06/17/15 Pct Recovery = 83% Analysis Date = 06/12/15 Pct Recovery = 84% Analysis Date = 06/12/15 Pct Recovery = 84% Analysis Date = 06/07/15 Pct Recovery = 84% Analysis Date = 06/07/15 Pct Recovery = 84% Analysis Date = 06/02/15 Pct Recovery = 84% Analysis Date = 06/02/15 Pct Recovery = 84% Analysis Date = 05/28/15 Pct Recovery = 85% Analysis Date = 05/28/15 Pct Recovery = 85% Analysis Date = 05/23/15 Pct Recovery = 85% Analysis Date = 05/23/15 Pct Recovery = 85% Analysis Date = 05/18/15 Pct Recovery = 85% Analysis Date = 05/18/15 Pct Recovery = 85% Analysis Date = 05/13/15 Pct Recovery = 86% Analysis Date = 05/13/15 Pct Recovery = 86% Analysis Date = 05/08/15 Pct Recovery = 86% Analysis Date = 05/08/15 Pct Recovery = 86% Analysis Date = 05/04/15 Pct Recovery = 86% Analysis Date = 05/04/15 Pct Recovery = 86% Analysis Date = 04/29/15 Pct Recovery = 87% Analysis Date = 04/29/15 Pct Recovery = 87% Analysis Date = 04/24/15 Pct Recovery = 87% Analysis Date = 04/24/15 Pct Recovery = 87% Analysis Date = 04/19/15 Pct Recovery = 87% Analysis Date = 04/19/15 Pct Recovery = 87% Analysis Date = 04/14/15 Pct Recovery = 87% Analysis Date = 04/14/15 Pct Recovery = 87% Analysis Date = 04/09/15 Pct Recovery = 88% Analysis Date = 04/09/15 Pct Recovery = 88% Analysis Date = 04/04/15 Pct Recovery = 88% Analysis Date = 04/04/15 Pct Recovery = 88% Analysis Date = 03/30/15 Pct Recovery = 88% Analysis Date = 03/30/15 Pct Recovery = 88% Analysis Date = 03/25/15 Pct Recovery = 88% Analysis Date = 03/25/15 Pct Recovery = 88% Analysis Date = 03/21/15 Pct Recovery = 88% Analysis Date = 03/21/15 Pct Recovery = 88% Analysis Date = 03/16/15 Pct Recovery = 89% Analysis Date = 03/16/15 Pct Recovery = 89% Analysis Date = 03/11/15 Pct Recovery = 89% Analysis Date = 03/11/15 Pct Recovery = 89% Analysis Date = 03/06/15 Pct Recovery = 89% Analysis Date = 03/06/15 Pct Recovery = 89% Analysis Date = 03/01/15 Pct Recovery = 89% Analysis Date = 03/01/15 Pct Recovery = 89% Analysis Date = 02/24/15 Pct Recovery = 89% Analysis Date = 02/24/15 Pct Recovery = 89% Analysis Date = 02/19/15 Pct Recovery = 90% Analysis Date = 02/19/15 Pct Recovery = 90% Analysis Date = 02/14/15 Pct Recovery = 90% Analysis Date = 02/14/15 Pct Recovery = 90% Analysis Date = 02/09/15 Pct Recovery = 90% Analysis Date = 02/09/15 Pct Recovery = 90% Analysis Date = 02/05/15 Pct Recovery = 90% Analysis Date = 02/05/15 Pct Recovery = 90% Analysis Date = 01/31/15 Pct Recovery = 90% Analysis Date = 01/31/15 Pct Recovery = 90% Analysis Date = 01/26/15 Pct Recovery = 91% Analysis Date = 01/26/15 Pct Recovery = 91% Analysis Date = 01/21/15 Pct Recovery = 91% Analysis Date = 01/21/15 Pct Recovery = 91% Analysis Date = 01/16/15 Pct Recovery = 91% Analysis Date = 01/16/15 Pct Recovery = 91% Analysis Date = 01/11/15 Pct Recovery = 91% Analysis Date = 01/11/15 Pct Recovery = 91% Analysis Date = 01/06/15 Pct Recovery = 92% Analysis Date = 01/06/15 Pct Recovery = 92% Analysis Date = 01/01/15 Pct Recovery = 92% Analysis Date = 01/01/15 Pct Recovery = 92% Analysis Date = 12/27/14 Pct Recovery = 92% Analysis Date = 12/27/14 Pct Recovery = 92% Analysis Date = 12/23/14 Pct Recovery = 92% Analysis Date = 12/23/14 Pct Recovery = 92% Analysis Date = 12/18/14 Pct Recovery = 92% Analysis Date = 12/18/14 Pct Recovery = 92% Analysis Date = 12/13/14 Pct Recovery = 93% Analysis Date = 12/13/14 Pct Recovery = 93% Analysis Date = 12/08/14 Pct Recovery = 93% Analysis Date = 12/08/14 Pct Recovery = 93% Analysis Date = 12/03/14 Pct Recovery = 93% Analysis Date = 12/03/14 Pct Recovery = 93% Analysis Date = 11/28/14 Pct Recovery = 93% Analysis Date = 11/28/14 Pct Recovery = 93% Analysis Date = 11/23/14 Pct Recovery = 93% Analysis Date = 11/23/14 Pct Recovery = 93% Analysis Date = 11/18/14 Pct Recovery = 94% Analysis Date = 11/18/14 Pct Recovery = 94% Analysis Date = 11/13/14 Pct Recovery = 94% Analysis Date = 11/13/14 Pct Recovery = 94% Analysis Date = 11/09/14 Pct Recovery = 94% Analysis Date = 11/09/14 Pct Recovery = 94% Analysis Date = 11/04/14 Pct Recovery = 94% Analysis Date = 11/04/14 Pct Recovery = 94% Analysis Date = 10/30/14 Pct Recovery = 94% Analysis Date = 10/30/14 Pct Recovery = 94% Analysis Date = 10/25/14 Pct Recovery = 95% Analysis Date = 10/25/14 Pct Recovery = 95% Analysis Date = 10/20/14 Pct Recovery = 95% Analysis Date = 10/20/14 Pct Recovery = 95% Analysis Date = 10/15/14 Pct Recovery = 95% Analysis Date = 10/15/14 Pct Recovery = 95% Analysis Date = 10/10/14 Pct Recovery = 95% Analysis Date = 10/10/14 Pct Recovery = 95% Analysis Date = 10/05/14 Pct Recovery = 96% Analysis Date = 10/05/14 Pct Recovery = 96% Analysis Date = 09/30/14 Pct Recovery = 96% Analysis Date = 09/30/14 Pct Recovery = 96% Analysis Date = 09/26/14 Pct Recovery = 96% Analysis Date = 09/26/14 Pct Recovery = 96% Analysis Date = 09/21/14 Pct Recovery = 96% Analysis Date = 09/21/14 Pct Recovery = 96% Analysis Date = 09/16/14 Pct Recovery = 96% Analysis Date = 09/16/14 Pct Recovery = 96% Analysis Date = 09/11/14 Pct Recovery = 97% Analysis Date = 09/11/14 Pct Recovery = 97% Analysis Date = 09/06/14 Pct Recovery = 97% Analysis Date = 09/06/14 Pct Recovery = 97% Analysis Date = 09/01/14 Pct Recovery = 97% Analysis Date = 09/01/14 Pct Recovery = 97% Analysis Date = 08/27/14 Pct Recovery = 97% Analysis Date = 08/27/14 Pct Recovery = 97% Analysis Date = 08/22/14 Pct Recovery = 97% Analysis Date = 08/22/14 Pct Recovery = 97% Analysis Date = 08/17/14 Pct Recovery = 97% Analysis Date = 08/17/14 Pct Recovery = 97% Analysis Date = 08/13/14 Pct Recovery = 98% Analysis Date = 08/13/14 Pct Recovery = 98% Analysis Date = 08/08/14 Pct Recovery = 98% Analysis Date = 08/08/14 Pct Recovery = 98% Analysis Date = 08/03/14 Pct Recovery = 98% Analysis Date = 08/03/14 Pct Recovery = 98% Analysis Date = 07/29/14 Pct Recovery = 98% Analysis Date = 07/29/14 Pct Recovery = 98% Analysis Date = 07/24/14 Pct Recovery = 98% Analysis Date = 07/24/14 Pct Recovery = 98% Analysis Date = 07/19/14 Pct Recovery = 99% Analysis Date = 07/19/14 Pct Recovery = 99% Analysis Date = 07/14/14 Pct Recovery = 99% Analysis Date = 07/14/14 Pct Recovery = 99% Analysis Date = 07/09/14 Pct Recovery = 99% Analysis Date = 07/09/14 Pct Recovery = 99% Analysis Date = 07/04/14 Pct Recovery = 99% Analysis Date = 07/04/14 Pct Recovery = 99% Analysis Date = 06/30/14 Pct Recovery = 99% Analysis Date = 06/30/14 Pct Recovery = 99% Analysis Date = 06/25/14 Pct Recovery = 99% Analysis Date = 06/25/14 Pct Recovery = 99% Analysis Date = 06/20/14 Pct Recovery = 99% Analysis Date = 06/20/14 Pct Recovery = 99% Analysis Date = 06/15/14 Pct Recovery = 100% Analysis Date = 06/15/14 Pct Recovery = 100% Analysis Date = 06/10/14 Pct Recovery = 100% Analysis Date = 06/10/14 Pct Recovery = 100% Analysis Date = 06/05/14 Pct Recovery = 100% Analysis Date = 06/05/14 Pct Recovery = 100% Analysis Date = 05/31/14 Pct Recovery = 100% Analysis Date = 05/31/14 Pct Recovery = 100% Analysis Date = 05/26/14 Pct Recovery = 100% Analysis Date = 05/26/14 Pct Recovery = 100% Analysis Date = 05/21/14 Pct Recovery = 100% Analysis Date = 05/21/14 Pct Recovery = 100% Analysis Date = 05/17/14 Pct Recovery = 101% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
TRIMETHOPRIM

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 75 81% 20% 80% 20%
Total 75 81% 20% 80% 20%

Sample Statistics
TRIMETHOPRIM

Characteristic N % % Basis
Plotted 75 97% Spiked
Estimated Values 8 10% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 77 .  
False Negatives 2 3% 2 out of 77
Not Spiked 38 .  
False Positives 0 0% 0 out of 38

BQS OBSP Determination:
VALACYCLOVIR
METHOD: 2440 , TESTIDCODE: 67507LCM56
Open Data Set

Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 28% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 31% Analysis Date = 01/17/16 SpikeMix = ERA 0406-15-09: 80 µl & ERA 0406-15-07A: 80 µl Pct Recovery = 77% Analysis Date = 11/24/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 76% Analysis Date = 10/01/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 58% Analysis Date = 11/05/15 SpikeMix = ERA 0406-15-08: 80 µl & Abs 052215: 80 µl Pct Recovery = 28% Analysis Date = 11/04/15 SpikeMix = Abs 052215: 80 µl & Abs 050115: 80 µl Pct Recovery = 21% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 26% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 31% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 45% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 44% Analysis Date = 05/07/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 51% Analysis Date = 04/29/15 SpikeMix = ERA 0319-14-05: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 45% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 49% Analysis Date = 01/16/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 49% Analysis Date = 12/07/14 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 43% Analysis Date = 12/06/14 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 40% Analysis Date = 08/28/14 SpikeMix = ERA 0319-14-04: 60 µl & ERA 0319-14-05: 60 µl Pct Recovery = 37% Analysis Date = 07/26/14 SpikeMix = ERA 0319-14-05: 60 µl & ERA 0318-14-02: 60 µl Pct Recovery = 3% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-04: 15 µl & Abs 041814: 15 µl Pct Recovery = 20% Analysis Date = 02/06/15 SpikeMix = Abs 041814: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 51% Analysis Date = 07/12/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 4% Analysis Date = 06/22/14 SpikeMix = Abs 041814: 60 µl & Abs 041614: 60 µl Pct Recovery = 6% Analysis Date = 05/21/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 4% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-08: 40 µl & ERA 0406-15-09: 40 µl Pct Recovery = 73% Analysis Date = 07/31/15 SpikeMix = ERA 0406-15-09: 40 µl & Abs 050115: 40 µl Pct Recovery = 74% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-08: 40 µl & Abs 052215: 40 µl Pct Recovery = 30% Analysis Date = 02/23/16 SpikeMix = Abs 052215: 40 µl & Abs 050115: 40 µl Pct Recovery = 28% Analysis Date = 09/10/15 SpikeMix = Abs 052215: 40 µl & ERA 0406-15-07A: 40 µl Pct Recovery = 25% Analysis Date = 07/31/15 SpikeMix = Abs 051315: 40 µl & Abs 052215: 40 µl Pct Recovery = 43% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 24% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 26% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 22% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 26% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 28% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 33% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 22% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 23% Analysis Date = 11/04/14 SpikeMix = Abs 041714: 8 µl & ERA 0319-14-05: 8 µl Pct Recovery = 50% Analysis Date = 10/24/14 SpikeMix = ERA 0319-14-05: 8 µl & Abs 041614: 8 µl Pct Recovery = 44% Analysis Date = 04/10/15 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 24% Analysis Date = 11/04/14 SpikeMix = Abs 041814: 8 µl & ERA 0318-14-02: 8 µl Pct Recovery = 35% Analysis Date = 10/11/14 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 56% Analysis Date = 08/30/14 SpikeMix = ERA 0318-14-02: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 23% Analysis Date = 08/16/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 5% Analysis Date = 07/13/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 3% Analysis Date = 10/10/14 SpikeMix = Abs 041714: 30 µl & Abs 041814: 30 µl Pct Recovery = 20% Analysis Date = 10/10/14 SpikeMix = Abs 041814: 30 µl & ERA 0318-14-02: 30 µl Pct Recovery = 14% Analysis Date = 07/13/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 3% Analysis Date = 05/30/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 5% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 82% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 24% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-08: 20 µl & ERA 0406-15-09: 20 µl Pct Recovery = 81% Analysis Date = 11/24/15 SpikeMix = ERA 0406-15-09: 20 µl & Abs 050115: 20 µl Pct Recovery = 53% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-09: 20 µl Pct Recovery = 42% Analysis Date = 11/24/15 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 35% Analysis Date = 09/09/15 SpikeMix = ERA 0406-15-08: 20 µl & Abs 052215: 20 µl Pct Recovery = 24% Analysis Date = 08/27/15 SpikeMix = Abs 052215: 20 µl & Abs 050115: 20 µl Pct Recovery = 37% Analysis Date = 07/09/15 SpikeMix = Abs 050115: 20 µl & Abs 052215: 20 µl Pct Recovery = 37% Analysis Date = 06/26/15 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 44% Analysis Date = 01/18/17 Pct Recovery = 23% Analysis Date = 01/14/17 Pct Recovery = 23% Analysis Date = 01/14/17 Pct Recovery = 23% Analysis Date = 01/09/17 Pct Recovery = 23% Analysis Date = 01/09/17 Pct Recovery = 23% Analysis Date = 01/04/17 Pct Recovery = 24% Analysis Date = 01/04/17 Pct Recovery = 24% Analysis Date = 12/30/16 Pct Recovery = 24% Analysis Date = 12/30/16 Pct Recovery = 24% Analysis Date = 12/25/16 Pct Recovery = 24% Analysis Date = 12/25/16 Pct Recovery = 24% Analysis Date = 12/20/16 Pct Recovery = 25% Analysis Date = 12/20/16 Pct Recovery = 25% Analysis Date = 12/15/16 Pct Recovery = 25% Analysis Date = 12/15/16 Pct Recovery = 25% Analysis Date = 12/11/16 Pct Recovery = 25% Analysis Date = 12/11/16 Pct Recovery = 25% Analysis Date = 12/06/16 Pct Recovery = 25% Analysis Date = 12/06/16 Pct Recovery = 25% Analysis Date = 12/01/16 Pct Recovery = 26% Analysis Date = 12/01/16 Pct Recovery = 26% Analysis Date = 11/26/16 Pct Recovery = 26% Analysis Date = 11/26/16 Pct Recovery = 26% Analysis Date = 11/21/16 Pct Recovery = 26% Analysis Date = 11/21/16 Pct Recovery = 26% Analysis Date = 11/16/16 Pct Recovery = 27% Analysis Date = 11/16/16 Pct Recovery = 27% Analysis Date = 11/11/16 Pct Recovery = 27% Analysis Date = 11/11/16 Pct Recovery = 27% Analysis Date = 11/06/16 Pct Recovery = 27% Analysis Date = 11/06/16 Pct Recovery = 27% Analysis Date = 11/02/16 Pct Recovery = 28% Analysis Date = 11/02/16 Pct Recovery = 28% Analysis Date = 10/28/16 Pct Recovery = 28% Analysis Date = 10/28/16 Pct Recovery = 28% Analysis Date = 10/23/16 Pct Recovery = 28% Analysis Date = 10/23/16 Pct Recovery = 28% Analysis Date = 10/18/16 Pct Recovery = 29% Analysis Date = 10/18/16 Pct Recovery = 29% Analysis Date = 10/13/16 Pct Recovery = 29% Analysis Date = 10/13/16 Pct Recovery = 29% Analysis Date = 10/08/16 Pct Recovery = 29% Analysis Date = 10/08/16 Pct Recovery = 29% Analysis Date = 10/03/16 Pct Recovery = 29% Analysis Date = 10/03/16 Pct Recovery = 29% Analysis Date = 09/28/16 Pct Recovery = 30% Analysis Date = 09/28/16 Pct Recovery = 30% Analysis Date = 09/24/16 Pct Recovery = 30% Analysis Date = 09/24/16 Pct Recovery = 30% Analysis Date = 09/19/16 Pct Recovery = 30% Analysis Date = 09/19/16 Pct Recovery = 30% Analysis Date = 09/14/16 Pct Recovery = 31% Analysis Date = 09/14/16 Pct Recovery = 31% Analysis Date = 09/09/16 Pct Recovery = 31% Analysis Date = 09/09/16 Pct Recovery = 31% Analysis Date = 09/04/16 Pct Recovery = 31% Analysis Date = 09/04/16 Pct Recovery = 31% Analysis Date = 08/30/16 Pct Recovery = 32% Analysis Date = 08/30/16 Pct Recovery = 32% Analysis Date = 08/25/16 Pct Recovery = 32% Analysis Date = 08/25/16 Pct Recovery = 32% Analysis Date = 08/21/16 Pct Recovery = 32% Analysis Date = 08/21/16 Pct Recovery = 32% Analysis Date = 08/16/16 Pct Recovery = 33% Analysis Date = 08/16/16 Pct Recovery = 33% Analysis Date = 08/11/16 Pct Recovery = 33% Analysis Date = 08/11/16 Pct Recovery = 33% Analysis Date = 08/06/16 Pct Recovery = 33% Analysis Date = 08/06/16 Pct Recovery = 33% Analysis Date = 08/01/16 Pct Recovery = 33% Analysis Date = 08/01/16 Pct Recovery = 33% Analysis Date = 07/27/16 Pct Recovery = 34% Analysis Date = 07/27/16 Pct Recovery = 34% Analysis Date = 07/22/16 Pct Recovery = 34% Analysis Date = 07/22/16 Pct Recovery = 34% Analysis Date = 07/17/16 Pct Recovery = 34% Analysis Date = 07/17/16 Pct Recovery = 34% Analysis Date = 07/13/16 Pct Recovery = 35% Analysis Date = 07/13/16 Pct Recovery = 35% Analysis Date = 07/08/16 Pct Recovery = 35% Analysis Date = 07/08/16 Pct Recovery = 35% Analysis Date = 07/03/16 Pct Recovery = 35% Analysis Date = 07/03/16 Pct Recovery = 35% Analysis Date = 06/28/16 Pct Recovery = 35% Analysis Date = 06/28/16 Pct Recovery = 35% Analysis Date = 06/23/16 Pct Recovery = 36% Analysis Date = 06/23/16 Pct Recovery = 36% Analysis Date = 06/18/16 Pct Recovery = 36% Analysis Date = 06/18/16 Pct Recovery = 36% Analysis Date = 06/13/16 Pct Recovery = 36% Analysis Date = 06/13/16 Pct Recovery = 36% Analysis Date = 06/08/16 Pct Recovery = 37% Analysis Date = 06/08/16 Pct Recovery = 37% Analysis Date = 06/04/16 Pct Recovery = 37% Analysis Date = 06/04/16 Pct Recovery = 37% Analysis Date = 05/30/16 Pct Recovery = 37% Analysis Date = 05/30/16 Pct Recovery = 37% Analysis Date = 05/25/16 Pct Recovery = 37% Analysis Date = 05/25/16 Pct Recovery = 37% Analysis Date = 05/20/16 Pct Recovery = 38% Analysis Date = 05/20/16 Pct Recovery = 38% Analysis Date = 05/15/16 Pct Recovery = 38% Analysis Date = 05/15/16 Pct Recovery = 38% Analysis Date = 05/10/16 Pct Recovery = 38% Analysis Date = 05/10/16 Pct Recovery = 38% Analysis Date = 05/05/16 Pct Recovery = 38% Analysis Date = 05/05/16 Pct Recovery = 38% Analysis Date = 05/01/16 Pct Recovery = 39% Analysis Date = 05/01/16 Pct Recovery = 39% Analysis Date = 04/26/16 Pct Recovery = 39% Analysis Date = 04/26/16 Pct Recovery = 39% Analysis Date = 04/21/16 Pct Recovery = 39% Analysis Date = 04/21/16 Pct Recovery = 39% Analysis Date = 04/16/16 Pct Recovery = 40% Analysis Date = 04/16/16 Pct Recovery = 40% Analysis Date = 04/11/16 Pct Recovery = 40% Analysis Date = 04/11/16 Pct Recovery = 40% Analysis Date = 04/06/16 Pct Recovery = 40% Analysis Date = 04/06/16 Pct Recovery = 40% Analysis Date = 04/01/16 Pct Recovery = 40% Analysis Date = 04/01/16 Pct Recovery = 40% Analysis Date = 03/27/16 Pct Recovery = 41% Analysis Date = 03/27/16 Pct Recovery = 41% Analysis Date = 03/23/16 Pct Recovery = 41% Analysis Date = 03/23/16 Pct Recovery = 41% Analysis Date = 03/18/16 Pct Recovery = 41% Analysis Date = 03/18/16 Pct Recovery = 41% Analysis Date = 03/13/16 Pct Recovery = 42% Analysis Date = 03/13/16 Pct Recovery = 42% Analysis Date = 03/08/16 Pct Recovery = 42% Analysis Date = 03/08/16 Pct Recovery = 42% Analysis Date = 03/03/16 Pct Recovery = 42% Analysis Date = 03/03/16 Pct Recovery = 42% Analysis Date = 02/27/16 Pct Recovery = 42% Analysis Date = 02/27/16 Pct Recovery = 42% Analysis Date = 02/22/16 Pct Recovery = 43% Analysis Date = 02/22/16 Pct Recovery = 43% Analysis Date = 02/17/16 Pct Recovery = 43% Analysis Date = 02/17/16 Pct Recovery = 43% Analysis Date = 02/13/16 Pct Recovery = 43% Analysis Date = 02/13/16 Pct Recovery = 43% Analysis Date = 02/08/16 Pct Recovery = 43% Analysis Date = 02/08/16 Pct Recovery = 43% Analysis Date = 02/03/16 Pct Recovery = 44% Analysis Date = 02/03/16 Pct Recovery = 44% Analysis Date = 01/29/16 Pct Recovery = 44% Analysis Date = 01/29/16 Pct Recovery = 44% Analysis Date = 01/24/16 Pct Recovery = 44% Analysis Date = 01/24/16 Pct Recovery = 44% Analysis Date = 01/19/16 Pct Recovery = 44% Analysis Date = 01/19/16 Pct Recovery = 44% Analysis Date = 01/14/16 Pct Recovery = 45% Analysis Date = 01/14/16 Pct Recovery = 45% Analysis Date = 01/10/16 Pct Recovery = 45% Analysis Date = 01/10/16 Pct Recovery = 45% Analysis Date = 01/05/16 Pct Recovery = 45% Analysis Date = 01/05/16 Pct Recovery = 45% Analysis Date = 12/31/15 Pct Recovery = 46% Analysis Date = 12/31/15 Pct Recovery = 46% Analysis Date = 12/26/15 Pct Recovery = 46% Analysis Date = 12/26/15 Pct Recovery = 46% Analysis Date = 12/21/15 Pct Recovery = 46% Analysis Date = 12/21/15 Pct Recovery = 46% Analysis Date = 12/16/15 Pct Recovery = 46% Analysis Date = 12/16/15 Pct Recovery = 46% Analysis Date = 12/11/15 Pct Recovery = 47% Analysis Date = 12/11/15 Pct Recovery = 47% Analysis Date = 12/06/15 Pct Recovery = 47% Analysis Date = 12/06/15 Pct Recovery = 47% Analysis Date = 12/02/15 Pct Recovery = 47% Analysis Date = 12/02/15 Pct Recovery = 47% Analysis Date = 11/27/15 Pct Recovery = 47% Analysis Date = 11/27/15 Pct Recovery = 47% Analysis Date = 11/22/15 Pct Recovery = 47% Analysis Date = 11/22/15 Pct Recovery = 47% Analysis Date = 11/17/15 Pct Recovery = 47% Analysis Date = 11/17/15 Pct Recovery = 47% Analysis Date = 11/12/15 Pct Recovery = 47% Analysis Date = 11/12/15 Pct Recovery = 47% Analysis Date = 11/07/15 Pct Recovery = 47% Analysis Date = 11/07/15 Pct Recovery = 47% Analysis Date = 11/02/15 Pct Recovery = 47% Analysis Date = 11/02/15 Pct Recovery = 47% Analysis Date = 10/28/15 Pct Recovery = 47% Analysis Date = 10/28/15 Pct Recovery = 47% Analysis Date = 10/24/15 Pct Recovery = 47% Analysis Date = 10/24/15 Pct Recovery = 47% Analysis Date = 10/19/15 Pct Recovery = 47% Analysis Date = 10/19/15 Pct Recovery = 47% Analysis Date = 10/14/15 Pct Recovery = 47% Analysis Date = 10/14/15 Pct Recovery = 47% Analysis Date = 10/09/15 Pct Recovery = 46% Analysis Date = 10/09/15 Pct Recovery = 46% Analysis Date = 10/04/15 Pct Recovery = 46% Analysis Date = 10/04/15 Pct Recovery = 46% Analysis Date = 09/29/15 Pct Recovery = 46% Analysis Date = 09/29/15 Pct Recovery = 46% Analysis Date = 09/24/15 Pct Recovery = 46% Analysis Date = 09/24/15 Pct Recovery = 46% Analysis Date = 09/19/15 Pct Recovery = 46% Analysis Date = 09/19/15 Pct Recovery = 46% Analysis Date = 09/15/15 Pct Recovery = 46% Analysis Date = 09/15/15 Pct Recovery = 46% Analysis Date = 09/10/15 Pct Recovery = 46% Analysis Date = 09/10/15 Pct Recovery = 46% Analysis Date = 09/05/15 Pct Recovery = 46% Analysis Date = 09/05/15 Pct Recovery = 46% Analysis Date = 08/31/15 Pct Recovery = 46% Analysis Date = 08/31/15 Pct Recovery = 46% Analysis Date = 08/26/15 Pct Recovery = 45% Analysis Date = 08/26/15 Pct Recovery = 45% Analysis Date = 08/21/15 Pct Recovery = 45% Analysis Date = 08/21/15 Pct Recovery = 45% Analysis Date = 08/16/15 Pct Recovery = 45% Analysis Date = 08/16/15 Pct Recovery = 45% Analysis Date = 08/12/15 Pct Recovery = 45% Analysis Date = 08/12/15 Pct Recovery = 45% Analysis Date = 08/07/15 Pct Recovery = 45% Analysis Date = 08/07/15 Pct Recovery = 45% Analysis Date = 08/02/15 Pct Recovery = 45% Analysis Date = 08/02/15 Pct Recovery = 45% Analysis Date = 07/28/15 Pct Recovery = 45% Analysis Date = 07/28/15 Pct Recovery = 45% Analysis Date = 07/23/15 Pct Recovery = 45% Analysis Date = 07/23/15 Pct Recovery = 45% Analysis Date = 07/18/15 Pct Recovery = 44% Analysis Date = 07/18/15 Pct Recovery = 44% Analysis Date = 07/13/15 Pct Recovery = 44% Analysis Date = 07/13/15 Pct Recovery = 44% Analysis Date = 07/08/15 Pct Recovery = 44% Analysis Date = 07/08/15 Pct Recovery = 44% Analysis Date = 07/04/15 Pct Recovery = 44% Analysis Date = 07/04/15 Pct Recovery = 44% Analysis Date = 06/29/15 Pct Recovery = 44% Analysis Date = 06/29/15 Pct Recovery = 44% Analysis Date = 06/24/15 Pct Recovery = 44% Analysis Date = 06/24/15 Pct Recovery = 44% Analysis Date = 06/19/15 Pct Recovery = 44% Analysis Date = 06/19/15 Pct Recovery = 44% Analysis Date = 06/14/15 Pct Recovery = 44% Analysis Date = 06/14/15 Pct Recovery = 44% Analysis Date = 06/09/15 Pct Recovery = 43% Analysis Date = 06/09/15 Pct Recovery = 43% Analysis Date = 06/04/15 Pct Recovery = 43% Analysis Date = 06/04/15 Pct Recovery = 43% Analysis Date = 05/30/15 Pct Recovery = 43% Analysis Date = 05/30/15 Pct Recovery = 43% Analysis Date = 05/26/15 Pct Recovery = 43% Analysis Date = 05/26/15 Pct Recovery = 43% Analysis Date = 05/21/15 Pct Recovery = 43% Analysis Date = 05/21/15 Pct Recovery = 43% Analysis Date = 05/16/15 Pct Recovery = 43% Analysis Date = 05/16/15 Pct Recovery = 43% Analysis Date = 05/11/15 Pct Recovery = 43% Analysis Date = 05/11/15 Pct Recovery = 43% Analysis Date = 05/06/15 Pct Recovery = 42% Analysis Date = 05/06/15 Pct Recovery = 42% Analysis Date = 05/01/15 Pct Recovery = 42% Analysis Date = 05/01/15 Pct Recovery = 42% Analysis Date = 04/26/15 Pct Recovery = 42% Analysis Date = 04/26/15 Pct Recovery = 42% Analysis Date = 04/22/15 Pct Recovery = 42% Analysis Date = 04/22/15 Pct Recovery = 42% Analysis Date = 04/17/15 Pct Recovery = 42% Analysis Date = 04/17/15 Pct Recovery = 42% Analysis Date = 04/12/15 Pct Recovery = 42% Analysis Date = 04/12/15 Pct Recovery = 42% Analysis Date = 04/07/15 Pct Recovery = 42% Analysis Date = 04/07/15 Pct Recovery = 42% Analysis Date = 04/02/15 Pct Recovery = 41% Analysis Date = 04/02/15 Pct Recovery = 41% Analysis Date = 03/28/15 Pct Recovery = 41% Analysis Date = 03/28/15 Pct Recovery = 41% Analysis Date = 03/23/15 Pct Recovery = 41% Analysis Date = 03/23/15 Pct Recovery = 41% Analysis Date = 03/18/15 Pct Recovery = 40% Analysis Date = 03/18/15 Pct Recovery = 40% Analysis Date = 03/14/15 Pct Recovery = 40% Analysis Date = 03/14/15 Pct Recovery = 40% Analysis Date = 03/09/15 Pct Recovery = 40% Analysis Date = 03/09/15 Pct Recovery = 40% Analysis Date = 03/04/15 Pct Recovery = 39% Analysis Date = 03/04/15 Pct Recovery = 39% Analysis Date = 02/27/15 Pct Recovery = 39% Analysis Date = 02/27/15 Pct Recovery = 39% Analysis Date = 02/22/15 Pct Recovery = 39% Analysis Date = 02/22/15 Pct Recovery = 39% Analysis Date = 02/17/15 Pct Recovery = 39% Analysis Date = 02/17/15 Pct Recovery = 39% Analysis Date = 02/12/15 Pct Recovery = 38% Analysis Date = 02/12/15 Pct Recovery = 38% Analysis Date = 02/07/15 Pct Recovery = 38% Analysis Date = 02/07/15 Pct Recovery = 38% Analysis Date = 02/03/15 Pct Recovery = 38% Analysis Date = 02/03/15 Pct Recovery = 38% Analysis Date = 01/29/15 Pct Recovery = 37% Analysis Date = 01/29/15 Pct Recovery = 37% Analysis Date = 01/24/15 Pct Recovery = 37% Analysis Date = 01/24/15 Pct Recovery = 37% Analysis Date = 01/19/15 Pct Recovery = 37% Analysis Date = 01/19/15 Pct Recovery = 37% Analysis Date = 01/14/15 Pct Recovery = 36% Analysis Date = 01/14/15 Pct Recovery = 36% Analysis Date = 01/09/15 Pct Recovery = 36% Analysis Date = 01/09/15 Pct Recovery = 36% Analysis Date = 01/04/15 Pct Recovery = 35% Analysis Date = 01/04/15 Pct Recovery = 35% Analysis Date = 12/31/14 Pct Recovery = 35% Analysis Date = 12/31/14 Pct Recovery = 35% Analysis Date = 12/26/14 Pct Recovery = 34% Analysis Date = 12/26/14 Pct Recovery = 34% Analysis Date = 12/21/14 Pct Recovery = 34% Analysis Date = 12/21/14 Pct Recovery = 34% Analysis Date = 12/16/14 Pct Recovery = 33% Analysis Date = 12/16/14 Pct Recovery = 33% Analysis Date = 12/11/14 Pct Recovery = 32% Analysis Date = 12/11/14 Pct Recovery = 32% Analysis Date = 12/06/14 Pct Recovery = 32% Analysis Date = 12/06/14 Pct Recovery = 32% Analysis Date = 12/01/14 Pct Recovery = 31% Analysis Date = 12/01/14 Pct Recovery = 31% Analysis Date = 11/26/14 Pct Recovery = 31% Analysis Date = 11/26/14 Pct Recovery = 31% Analysis Date = 11/22/14 Pct Recovery = 30% Analysis Date = 11/22/14 Pct Recovery = 30% Analysis Date = 11/17/14 Pct Recovery = 30% Analysis Date = 11/17/14 Pct Recovery = 30% Analysis Date = 11/12/14 Pct Recovery = 29% Analysis Date = 11/12/14 Pct Recovery = 29% Analysis Date = 11/07/14 Pct Recovery = 29% Analysis Date = 11/07/14 Pct Recovery = 29% Analysis Date = 11/02/14 Pct Recovery = 28% Analysis Date = 11/02/14 Pct Recovery = 28% Analysis Date = 10/28/14 Pct Recovery = 27% Analysis Date = 10/28/14 Pct Recovery = 27% Analysis Date = 10/23/14 Pct Recovery = 27% Analysis Date = 10/23/14 Pct Recovery = 27% Analysis Date = 10/18/14 Pct Recovery = 26% Analysis Date = 10/18/14 Pct Recovery = 26% Analysis Date = 10/14/14 Pct Recovery = 26% Analysis Date = 10/14/14 Pct Recovery = 26% Analysis Date = 10/09/14 Pct Recovery = 25% Analysis Date = 10/09/14 Pct Recovery = 25% Analysis Date = 10/04/14 Pct Recovery = 24% Analysis Date = 10/04/14 Pct Recovery = 24% Analysis Date = 09/29/14 Pct Recovery = 24% Analysis Date = 09/29/14 Pct Recovery = 24% Analysis Date = 09/24/14 Pct Recovery = 23% Analysis Date = 09/24/14 Pct Recovery = 23% Analysis Date = 09/19/14 Pct Recovery = 23% Analysis Date = 09/19/14 Pct Recovery = 23% Analysis Date = 09/14/14 Pct Recovery = 22% Analysis Date = 09/14/14 Pct Recovery = 22% Analysis Date = 09/10/14 Pct Recovery = 21% Analysis Date = 09/10/14 Pct Recovery = 21% Analysis Date = 09/05/14 Pct Recovery = 21% Analysis Date = 09/05/14 Pct Recovery = 21% Analysis Date = 08/31/14 Pct Recovery = 20% Analysis Date = 08/31/14 Pct Recovery = 20% Analysis Date = 08/26/14 Pct Recovery = 20% Analysis Date = 08/26/14 Pct Recovery = 20% Analysis Date = 08/21/14 Pct Recovery = 19% Analysis Date = 08/21/14 Pct Recovery = 19% Analysis Date = 08/16/14 Pct Recovery = 18% Analysis Date = 08/16/14 Pct Recovery = 18% Analysis Date = 08/11/14 Pct Recovery = 18% Analysis Date = 08/11/14 Pct Recovery = 18% Analysis Date = 08/06/14 Pct Recovery = 17% Analysis Date = 08/06/14 Pct Recovery = 17% Analysis Date = 08/02/14 Pct Recovery = 17% Analysis Date = 08/02/14 Pct Recovery = 17% Analysis Date = 07/28/14 Pct Recovery = 16% Analysis Date = 07/28/14 Pct Recovery = 16% Analysis Date = 07/23/14 Pct Recovery = 15% Analysis Date = 07/23/14 Pct Recovery = 15% Analysis Date = 07/18/14 Pct Recovery = 15% Analysis Date = 07/18/14 Pct Recovery = 15% Analysis Date = 07/13/14 Pct Recovery = 14% Analysis Date = 07/13/14 Pct Recovery = 14% Analysis Date = 07/08/14 Pct Recovery = 13% Analysis Date = 07/08/14 Pct Recovery = 13% Analysis Date = 07/03/14 Pct Recovery = 13% Analysis Date = 07/03/14 Pct Recovery = 13% Analysis Date = 06/28/14 Pct Recovery = 12% Analysis Date = 06/28/14 Pct Recovery = 12% Analysis Date = 06/24/14 Pct Recovery = 11% Analysis Date = 06/24/14 Pct Recovery = 11% Analysis Date = 06/19/14 Pct Recovery = 11% Analysis Date = 06/19/14 Pct Recovery = 11% Analysis Date = 06/14/14 Pct Recovery = 10% Analysis Date = 06/14/14 Pct Recovery = 10% Analysis Date = 06/09/14 Pct Recovery = 9% Analysis Date = 06/09/14 Pct Recovery = 9% Analysis Date = 06/04/14 Pct Recovery = 8% Analysis Date = 06/04/14 Pct Recovery = 8% Analysis Date = 05/30/14 Pct Recovery = 8% Analysis Date = 05/30/14 Pct Recovery = 8% Analysis Date = 05/25/14 Pct Recovery = 7% Analysis Date = 05/25/14 Pct Recovery = 7% Analysis Date = 05/21/14 Pct Recovery = 6% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
VALACYCLOVIR

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 60 35% 20% 31% 16%
Total 60 35% 20% 31% 16%

Sample Statistics
VALACYCLOVIR

Characteristic N % % Basis
Plotted 60 92% Spiked
Estimated Values 60 92% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 2 3% Spiked
Spiked 65 .  
False Negatives 3 5% 3 out of 65
Not Spiked 50 .  
False Positives 0 0% 0 out of 50

BQS OBSP Determination:
VENLAFAXINE
METHOD: 2440 , TESTIDCODE: 67534LCM56
Open Data Set

Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 66% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 69% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 80 µl & ERA 0406-15-08: 80 µl Pct Recovery = 62% Analysis Date = 11/05/15 SpikeMix = ERA 0406-15-08: 80 µl & Abs 052215: 80 µl Pct Recovery = 64% Analysis Date = 11/24/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 81% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 80 µl & Abs 051315: 80 µl Pct Recovery = 98% Analysis Date = 10/01/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 87% Analysis Date = 11/18/16 SpikeMix = ERA 04281604: 80 µl & ERA 04281603: 80 µl Pct Recovery = 62% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & ERA 04281604: 80 µl Pct Recovery = 59% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 55% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 57% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 58% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 65% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 78% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 75% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-04: 15 µl & Abs 041814: 15 µl Pct Recovery = 70% Analysis Date = 02/06/15 SpikeMix = Abs 041814: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 76% Analysis Date = 07/12/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 67% Analysis Date = 06/22/14 SpikeMix = Abs 041814: 60 µl & Abs 041614: 60 µl Pct Recovery = 89% Analysis Date = 05/21/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 72% Analysis Date = 05/07/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 90% Analysis Date = 04/29/15 SpikeMix = ERA 0319-14-05: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 61% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 74% Analysis Date = 01/16/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 78% Analysis Date = 12/07/14 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 66% Analysis Date = 12/06/14 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 64% Analysis Date = 08/28/14 SpikeMix = ERA 0319-14-04: 60 µl & ERA 0319-14-05: 60 µl Pct Recovery = 57% Analysis Date = 07/26/14 SpikeMix = ERA 0319-14-05: 60 µl & ERA 0318-14-02: 60 µl Pct Recovery = 75% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-08: 40 µl & Abs 052215: 40 µl Pct Recovery = 59% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 62% Analysis Date = 11/04/15 SpikeMix = ERA 0406-15-07A: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 61% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-08: 40 µl & ERA 0406-15-09: 40 µl Pct Recovery = 64% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 48% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 40% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-07A: 40 µl & Abs 051315: 40 µl Pct Recovery = 45% Analysis Date = 07/31/15 SpikeMix = Abs 051315: 40 µl & Abs 052215: 40 µl Pct Recovery = 50% Analysis Date = 07/30/15 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 64% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 58% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 63% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 51% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 56% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 94% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 99% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 72% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 75% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 66% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 76% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 49% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 57% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 49% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 55% Analysis Date = 04/10/15 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 65% Analysis Date = 10/11/14 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 48% Analysis Date = 10/24/14 SpikeMix = ERA 0319-14-05: 8 µl & Abs 041614: 8 µl Pct Recovery = 75% Analysis Date = 10/10/14 SpikeMix = Abs 041714: 30 µl & Abs 041814: 30 µl Pct Recovery = 55% Analysis Date = 10/10/14 SpikeMix = Abs 041814: 30 µl & ERA 0318-14-02: 30 µl Pct Recovery = 50% Analysis Date = 07/13/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 56% Analysis Date = 05/30/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 63% Analysis Date = 08/30/14 SpikeMix = ERA 0318-14-02: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 76% Analysis Date = 08/16/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 39% Analysis Date = 07/13/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 46% Analysis Date = 04/27/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 79% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 56% Analysis Date = 11/25/15 SpikeMix = Abs 050115: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 74% Analysis Date = 09/15/15 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 55% Analysis Date = 02/23/16 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 51% Analysis Date = 08/11/15 SpikeMix = Abs 050115: 20 µl & Abs 051315: 20 µl Pct Recovery = 47% Analysis Date = 06/26/15 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 54% Analysis Date = 04/09/16 SpikeMix = Abs 051315: 10 µl & ERA 0406-15-09: 10 µl Pct Recovery = 64% Analysis Date = 01/18/17 Pct Recovery = 71% Analysis Date = 01/14/17 Pct Recovery = 71% Analysis Date = 01/14/17 Pct Recovery = 71% Analysis Date = 01/09/17 Pct Recovery = 71% Analysis Date = 01/09/17 Pct Recovery = 71% Analysis Date = 01/04/17 Pct Recovery = 70% Analysis Date = 01/04/17 Pct Recovery = 70% Analysis Date = 12/30/16 Pct Recovery = 70% Analysis Date = 12/30/16 Pct Recovery = 70% Analysis Date = 12/25/16 Pct Recovery = 70% Analysis Date = 12/25/16 Pct Recovery = 70% Analysis Date = 12/20/16 Pct Recovery = 69% Analysis Date = 12/20/16 Pct Recovery = 69% Analysis Date = 12/15/16 Pct Recovery = 69% Analysis Date = 12/15/16 Pct Recovery = 69% Analysis Date = 12/11/16 Pct Recovery = 69% Analysis Date = 12/11/16 Pct Recovery = 69% Analysis Date = 12/06/16 Pct Recovery = 69% Analysis Date = 12/06/16 Pct Recovery = 69% Analysis Date = 12/01/16 Pct Recovery = 68% Analysis Date = 12/01/16 Pct Recovery = 68% Analysis Date = 11/26/16 Pct Recovery = 68% Analysis Date = 11/26/16 Pct Recovery = 68% Analysis Date = 11/21/16 Pct Recovery = 68% Analysis Date = 11/21/16 Pct Recovery = 68% Analysis Date = 11/16/16 Pct Recovery = 67% Analysis Date = 11/16/16 Pct Recovery = 67% Analysis Date = 11/11/16 Pct Recovery = 67% Analysis Date = 11/11/16 Pct Recovery = 67% Analysis Date = 11/06/16 Pct Recovery = 67% Analysis Date = 11/06/16 Pct Recovery = 67% Analysis Date = 11/02/16 Pct Recovery = 67% Analysis Date = 11/02/16 Pct Recovery = 67% Analysis Date = 10/28/16 Pct Recovery = 66% Analysis Date = 10/28/16 Pct Recovery = 66% Analysis Date = 10/23/16 Pct Recovery = 66% Analysis Date = 10/23/16 Pct Recovery = 66% Analysis Date = 10/18/16 Pct Recovery = 66% Analysis Date = 10/18/16 Pct Recovery = 66% Analysis Date = 10/13/16 Pct Recovery = 66% Analysis Date = 10/13/16 Pct Recovery = 66% Analysis Date = 10/08/16 Pct Recovery = 65% Analysis Date = 10/08/16 Pct Recovery = 65% Analysis Date = 10/03/16 Pct Recovery = 65% Analysis Date = 10/03/16 Pct Recovery = 65% Analysis Date = 09/28/16 Pct Recovery = 65% Analysis Date = 09/28/16 Pct Recovery = 65% Analysis Date = 09/24/16 Pct Recovery = 65% Analysis Date = 09/24/16 Pct Recovery = 65% Analysis Date = 09/19/16 Pct Recovery = 64% Analysis Date = 09/19/16 Pct Recovery = 64% Analysis Date = 09/14/16 Pct Recovery = 64% Analysis Date = 09/14/16 Pct Recovery = 64% Analysis Date = 09/09/16 Pct Recovery = 64% Analysis Date = 09/09/16 Pct Recovery = 64% Analysis Date = 09/04/16 Pct Recovery = 64% Analysis Date = 09/04/16 Pct Recovery = 64% Analysis Date = 08/30/16 Pct Recovery = 64% Analysis Date = 08/30/16 Pct Recovery = 64% Analysis Date = 08/25/16 Pct Recovery = 64% Analysis Date = 08/25/16 Pct Recovery = 64% Analysis Date = 08/21/16 Pct Recovery = 63% Analysis Date = 08/21/16 Pct Recovery = 63% Analysis Date = 08/16/16 Pct Recovery = 63% Analysis Date = 08/16/16 Pct Recovery = 63% Analysis Date = 08/11/16 Pct Recovery = 63% Analysis Date = 08/11/16 Pct Recovery = 63% Analysis Date = 08/06/16 Pct Recovery = 63% Analysis Date = 08/06/16 Pct Recovery = 63% Analysis Date = 08/01/16 Pct Recovery = 63% Analysis Date = 08/01/16 Pct Recovery = 63% Analysis Date = 07/27/16 Pct Recovery = 63% Analysis Date = 07/27/16 Pct Recovery = 63% Analysis Date = 07/22/16 Pct Recovery = 63% Analysis Date = 07/22/16 Pct Recovery = 63% Analysis Date = 07/17/16 Pct Recovery = 63% Analysis Date = 07/17/16 Pct Recovery = 63% Analysis Date = 07/13/16 Pct Recovery = 63% Analysis Date = 07/13/16 Pct Recovery = 63% Analysis Date = 07/08/16 Pct Recovery = 62% Analysis Date = 07/08/16 Pct Recovery = 62% Analysis Date = 07/03/16 Pct Recovery = 62% Analysis Date = 07/03/16 Pct Recovery = 62% Analysis Date = 06/28/16 Pct Recovery = 62% Analysis Date = 06/28/16 Pct Recovery = 62% Analysis Date = 06/23/16 Pct Recovery = 62% Analysis Date = 06/23/16 Pct Recovery = 62% Analysis Date = 06/18/16 Pct Recovery = 62% Analysis Date = 06/18/16 Pct Recovery = 62% Analysis Date = 06/13/16 Pct Recovery = 62% Analysis Date = 06/13/16 Pct Recovery = 62% Analysis Date = 06/08/16 Pct Recovery = 62% Analysis Date = 06/08/16 Pct Recovery = 62% Analysis Date = 06/04/16 Pct Recovery = 62% Analysis Date = 06/04/16 Pct Recovery = 62% Analysis Date = 05/30/16 Pct Recovery = 62% Analysis Date = 05/30/16 Pct Recovery = 62% Analysis Date = 05/25/16 Pct Recovery = 62% Analysis Date = 05/25/16 Pct Recovery = 62% Analysis Date = 05/20/16 Pct Recovery = 61% Analysis Date = 05/20/16 Pct Recovery = 61% Analysis Date = 05/15/16 Pct Recovery = 61% Analysis Date = 05/15/16 Pct Recovery = 61% Analysis Date = 05/10/16 Pct Recovery = 61% Analysis Date = 05/10/16 Pct Recovery = 61% Analysis Date = 05/05/16 Pct Recovery = 61% Analysis Date = 05/05/16 Pct Recovery = 61% Analysis Date = 05/01/16 Pct Recovery = 61% Analysis Date = 05/01/16 Pct Recovery = 61% Analysis Date = 04/26/16 Pct Recovery = 61% Analysis Date = 04/26/16 Pct Recovery = 61% Analysis Date = 04/21/16 Pct Recovery = 61% Analysis Date = 04/21/16 Pct Recovery = 61% Analysis Date = 04/16/16 Pct Recovery = 61% Analysis Date = 04/16/16 Pct Recovery = 61% Analysis Date = 04/11/16 Pct Recovery = 61% Analysis Date = 04/11/16 Pct Recovery = 61% Analysis Date = 04/06/16 Pct Recovery = 61% Analysis Date = 04/06/16 Pct Recovery = 61% Analysis Date = 04/01/16 Pct Recovery = 61% Analysis Date = 04/01/16 Pct Recovery = 61% Analysis Date = 03/27/16 Pct Recovery = 62% Analysis Date = 03/27/16 Pct Recovery = 62% Analysis Date = 03/23/16 Pct Recovery = 62% Analysis Date = 03/23/16 Pct Recovery = 62% Analysis Date = 03/18/16 Pct Recovery = 62% Analysis Date = 03/18/16 Pct Recovery = 62% Analysis Date = 03/13/16 Pct Recovery = 62% Analysis Date = 03/13/16 Pct Recovery = 62% Analysis Date = 03/08/16 Pct Recovery = 62% Analysis Date = 03/08/16 Pct Recovery = 62% Analysis Date = 03/03/16 Pct Recovery = 62% Analysis Date = 03/03/16 Pct Recovery = 62% Analysis Date = 02/27/16 Pct Recovery = 62% Analysis Date = 02/27/16 Pct Recovery = 62% Analysis Date = 02/22/16 Pct Recovery = 62% Analysis Date = 02/22/16 Pct Recovery = 62% Analysis Date = 02/17/16 Pct Recovery = 62% Analysis Date = 02/17/16 Pct Recovery = 62% Analysis Date = 02/13/16 Pct Recovery = 62% Analysis Date = 02/13/16 Pct Recovery = 62% Analysis Date = 02/08/16 Pct Recovery = 63% Analysis Date = 02/08/16 Pct Recovery = 63% Analysis Date = 02/03/16 Pct Recovery = 63% Analysis Date = 02/03/16 Pct Recovery = 63% Analysis Date = 01/29/16 Pct Recovery = 63% Analysis Date = 01/29/16 Pct Recovery = 63% Analysis Date = 01/24/16 Pct Recovery = 63% Analysis Date = 01/24/16 Pct Recovery = 63% Analysis Date = 01/19/16 Pct Recovery = 63% Analysis Date = 01/19/16 Pct Recovery = 63% Analysis Date = 01/14/16 Pct Recovery = 63% Analysis Date = 01/14/16 Pct Recovery = 63% Analysis Date = 01/10/16 Pct Recovery = 63% Analysis Date = 01/10/16 Pct Recovery = 63% Analysis Date = 01/05/16 Pct Recovery = 63% Analysis Date = 01/05/16 Pct Recovery = 63% Analysis Date = 12/31/15 Pct Recovery = 63% Analysis Date = 12/31/15 Pct Recovery = 63% Analysis Date = 12/26/15 Pct Recovery = 63% Analysis Date = 12/26/15 Pct Recovery = 63% Analysis Date = 12/21/15 Pct Recovery = 63% Analysis Date = 12/21/15 Pct Recovery = 63% Analysis Date = 12/16/15 Pct Recovery = 63% Analysis Date = 12/16/15 Pct Recovery = 63% Analysis Date = 12/11/15 Pct Recovery = 63% Analysis Date = 12/11/15 Pct Recovery = 63% Analysis Date = 12/06/15 Pct Recovery = 63% Analysis Date = 12/06/15 Pct Recovery = 63% Analysis Date = 12/02/15 Pct Recovery = 63% Analysis Date = 12/02/15 Pct Recovery = 63% Analysis Date = 11/27/15 Pct Recovery = 63% Analysis Date = 11/27/15 Pct Recovery = 63% Analysis Date = 11/22/15 Pct Recovery = 64% Analysis Date = 11/22/15 Pct Recovery = 64% Analysis Date = 11/17/15 Pct Recovery = 64% Analysis Date = 11/17/15 Pct Recovery = 64% Analysis Date = 11/12/15 Pct Recovery = 64% Analysis Date = 11/12/15 Pct Recovery = 64% Analysis Date = 11/07/15 Pct Recovery = 64% Analysis Date = 11/07/15 Pct Recovery = 64% Analysis Date = 11/02/15 Pct Recovery = 64% Analysis Date = 11/02/15 Pct Recovery = 64% Analysis Date = 10/28/15 Pct Recovery = 64% Analysis Date = 10/28/15 Pct Recovery = 64% Analysis Date = 10/24/15 Pct Recovery = 64% Analysis Date = 10/24/15 Pct Recovery = 64% Analysis Date = 10/19/15 Pct Recovery = 64% Analysis Date = 10/19/15 Pct Recovery = 64% Analysis Date = 10/14/15 Pct Recovery = 65% Analysis Date = 10/14/15 Pct Recovery = 65% Analysis Date = 10/09/15 Pct Recovery = 65% Analysis Date = 10/09/15 Pct Recovery = 65% Analysis Date = 10/04/15 Pct Recovery = 65% Analysis Date = 10/04/15 Pct Recovery = 65% Analysis Date = 09/29/15 Pct Recovery = 65% Analysis Date = 09/29/15 Pct Recovery = 65% Analysis Date = 09/24/15 Pct Recovery = 65% Analysis Date = 09/24/15 Pct Recovery = 65% Analysis Date = 09/19/15 Pct Recovery = 65% Analysis Date = 09/19/15 Pct Recovery = 65% Analysis Date = 09/15/15 Pct Recovery = 65% Analysis Date = 09/15/15 Pct Recovery = 65% Analysis Date = 09/10/15 Pct Recovery = 65% Analysis Date = 09/10/15 Pct Recovery = 65% Analysis Date = 09/05/15 Pct Recovery = 65% Analysis Date = 09/05/15 Pct Recovery = 65% Analysis Date = 08/31/15 Pct Recovery = 66% Analysis Date = 08/31/15 Pct Recovery = 66% Analysis Date = 08/26/15 Pct Recovery = 66% Analysis Date = 08/26/15 Pct Recovery = 66% Analysis Date = 08/21/15 Pct Recovery = 66% Analysis Date = 08/21/15 Pct Recovery = 66% Analysis Date = 08/16/15 Pct Recovery = 66% Analysis Date = 08/16/15 Pct Recovery = 66% Analysis Date = 08/12/15 Pct Recovery = 66% Analysis Date = 08/12/15 Pct Recovery = 66% Analysis Date = 08/07/15 Pct Recovery = 66% Analysis Date = 08/07/15 Pct Recovery = 66% Analysis Date = 08/02/15 Pct Recovery = 66% Analysis Date = 08/02/15 Pct Recovery = 66% Analysis Date = 07/28/15 Pct Recovery = 66% Analysis Date = 07/28/15 Pct Recovery = 66% Analysis Date = 07/23/15 Pct Recovery = 66% Analysis Date = 07/23/15 Pct Recovery = 66% Analysis Date = 07/18/15 Pct Recovery = 66% Analysis Date = 07/18/15 Pct Recovery = 66% Analysis Date = 07/13/15 Pct Recovery = 66% Analysis Date = 07/13/15 Pct Recovery = 66% Analysis Date = 07/08/15 Pct Recovery = 66% Analysis Date = 07/08/15 Pct Recovery = 66% Analysis Date = 07/04/15 Pct Recovery = 66% Analysis Date = 07/04/15 Pct Recovery = 66% Analysis Date = 06/29/15 Pct Recovery = 66% Analysis Date = 06/29/15 Pct Recovery = 66% Analysis Date = 06/24/15 Pct Recovery = 66% Analysis Date = 06/24/15 Pct Recovery = 66% Analysis Date = 06/19/15 Pct Recovery = 66% Analysis Date = 06/19/15 Pct Recovery = 66% Analysis Date = 06/14/15 Pct Recovery = 66% Analysis Date = 06/14/15 Pct Recovery = 66% Analysis Date = 06/09/15 Pct Recovery = 66% Analysis Date = 06/09/15 Pct Recovery = 66% Analysis Date = 06/04/15 Pct Recovery = 66% Analysis Date = 06/04/15 Pct Recovery = 66% Analysis Date = 05/30/15 Pct Recovery = 66% Analysis Date = 05/30/15 Pct Recovery = 66% Analysis Date = 05/26/15 Pct Recovery = 66% Analysis Date = 05/26/15 Pct Recovery = 66% Analysis Date = 05/21/15 Pct Recovery = 66% Analysis Date = 05/21/15 Pct Recovery = 66% Analysis Date = 05/16/15 Pct Recovery = 66% Analysis Date = 05/16/15 Pct Recovery = 66% Analysis Date = 05/11/15 Pct Recovery = 66% Analysis Date = 05/11/15 Pct Recovery = 66% Analysis Date = 05/06/15 Pct Recovery = 66% Analysis Date = 05/06/15 Pct Recovery = 66% Analysis Date = 05/01/15 Pct Recovery = 66% Analysis Date = 05/01/15 Pct Recovery = 66% Analysis Date = 04/26/15 Pct Recovery = 66% Analysis Date = 04/26/15 Pct Recovery = 66% Analysis Date = 04/22/15 Pct Recovery = 66% Analysis Date = 04/22/15 Pct Recovery = 66% Analysis Date = 04/17/15 Pct Recovery = 66% Analysis Date = 04/17/15 Pct Recovery = 66% Analysis Date = 04/12/15 Pct Recovery = 66% Analysis Date = 04/12/15 Pct Recovery = 66% Analysis Date = 04/07/15 Pct Recovery = 66% Analysis Date = 04/07/15 Pct Recovery = 66% Analysis Date = 04/02/15 Pct Recovery = 66% Analysis Date = 04/02/15 Pct Recovery = 66% Analysis Date = 03/28/15 Pct Recovery = 66% Analysis Date = 03/28/15 Pct Recovery = 66% Analysis Date = 03/23/15 Pct Recovery = 66% Analysis Date = 03/23/15 Pct Recovery = 66% Analysis Date = 03/18/15 Pct Recovery = 66% Analysis Date = 03/18/15 Pct Recovery = 66% Analysis Date = 03/14/15 Pct Recovery = 66% Analysis Date = 03/14/15 Pct Recovery = 66% Analysis Date = 03/09/15 Pct Recovery = 66% Analysis Date = 03/09/15 Pct Recovery = 66% Analysis Date = 03/04/15 Pct Recovery = 66% Analysis Date = 03/04/15 Pct Recovery = 66% Analysis Date = 02/27/15 Pct Recovery = 66% Analysis Date = 02/27/15 Pct Recovery = 66% Analysis Date = 02/22/15 Pct Recovery = 65% Analysis Date = 02/22/15 Pct Recovery = 65% Analysis Date = 02/17/15 Pct Recovery = 65% Analysis Date = 02/17/15 Pct Recovery = 65% Analysis Date = 02/12/15 Pct Recovery = 65% Analysis Date = 02/12/15 Pct Recovery = 65% Analysis Date = 02/07/15 Pct Recovery = 65% Analysis Date = 02/07/15 Pct Recovery = 65% Analysis Date = 02/03/15 Pct Recovery = 65% Analysis Date = 02/03/15 Pct Recovery = 65% Analysis Date = 01/29/15 Pct Recovery = 65% Analysis Date = 01/29/15 Pct Recovery = 65% Analysis Date = 01/24/15 Pct Recovery = 65% Analysis Date = 01/24/15 Pct Recovery = 65% Analysis Date = 01/19/15 Pct Recovery = 65% Analysis Date = 01/19/15 Pct Recovery = 65% Analysis Date = 01/14/15 Pct Recovery = 65% Analysis Date = 01/14/15 Pct Recovery = 65% Analysis Date = 01/09/15 Pct Recovery = 65% Analysis Date = 01/09/15 Pct Recovery = 65% Analysis Date = 01/04/15 Pct Recovery = 65% Analysis Date = 01/04/15 Pct Recovery = 65% Analysis Date = 12/31/14 Pct Recovery = 65% Analysis Date = 12/31/14 Pct Recovery = 65% Analysis Date = 12/26/14 Pct Recovery = 65% Analysis Date = 12/26/14 Pct Recovery = 65% Analysis Date = 12/21/14 Pct Recovery = 65% Analysis Date = 12/21/14 Pct Recovery = 65% Analysis Date = 12/16/14 Pct Recovery = 65% Analysis Date = 12/16/14 Pct Recovery = 65% Analysis Date = 12/11/14 Pct Recovery = 65% Analysis Date = 12/11/14 Pct Recovery = 65% Analysis Date = 12/06/14 Pct Recovery = 65% Analysis Date = 12/06/14 Pct Recovery = 65% Analysis Date = 12/01/14 Pct Recovery = 65% Analysis Date = 12/01/14 Pct Recovery = 65% Analysis Date = 11/26/14 Pct Recovery = 65% Analysis Date = 11/26/14 Pct Recovery = 65% Analysis Date = 11/22/14 Pct Recovery = 65% Analysis Date = 11/22/14 Pct Recovery = 65% Analysis Date = 11/17/14 Pct Recovery = 65% Analysis Date = 11/17/14 Pct Recovery = 65% Analysis Date = 11/12/14 Pct Recovery = 65% Analysis Date = 11/12/14 Pct Recovery = 65% Analysis Date = 11/07/14 Pct Recovery = 65% Analysis Date = 11/07/14 Pct Recovery = 65% Analysis Date = 11/02/14 Pct Recovery = 65% Analysis Date = 11/02/14 Pct Recovery = 65% Analysis Date = 10/28/14 Pct Recovery = 65% Analysis Date = 10/28/14 Pct Recovery = 65% Analysis Date = 10/23/14 Pct Recovery = 65% Analysis Date = 10/23/14 Pct Recovery = 65% Analysis Date = 10/18/14 Pct Recovery = 65% Analysis Date = 10/18/14 Pct Recovery = 65% Analysis Date = 10/14/14 Pct Recovery = 64% Analysis Date = 10/14/14 Pct Recovery = 64% Analysis Date = 10/09/14 Pct Recovery = 64% Analysis Date = 10/09/14 Pct Recovery = 64% Analysis Date = 10/04/14 Pct Recovery = 64% Analysis Date = 10/04/14 Pct Recovery = 64% Analysis Date = 09/29/14 Pct Recovery = 64% Analysis Date = 09/29/14 Pct Recovery = 64% Analysis Date = 09/24/14 Pct Recovery = 64% Analysis Date = 09/24/14 Pct Recovery = 64% Analysis Date = 09/19/14 Pct Recovery = 64% Analysis Date = 09/19/14 Pct Recovery = 64% Analysis Date = 09/14/14 Pct Recovery = 64% Analysis Date = 09/14/14 Pct Recovery = 64% Analysis Date = 09/10/14 Pct Recovery = 64% Analysis Date = 09/10/14 Pct Recovery = 64% Analysis Date = 09/05/14 Pct Recovery = 64% Analysis Date = 09/05/14 Pct Recovery = 64% Analysis Date = 08/31/14 Pct Recovery = 64% Analysis Date = 08/31/14 Pct Recovery = 64% Analysis Date = 08/26/14 Pct Recovery = 64% Analysis Date = 08/26/14 Pct Recovery = 64% Analysis Date = 08/21/14 Pct Recovery = 64% Analysis Date = 08/21/14 Pct Recovery = 64% Analysis Date = 08/16/14 Pct Recovery = 64% Analysis Date = 08/16/14 Pct Recovery = 64% Analysis Date = 08/11/14 Pct Recovery = 64% Analysis Date = 08/11/14 Pct Recovery = 64% Analysis Date = 08/06/14 Pct Recovery = 64% Analysis Date = 08/06/14 Pct Recovery = 64% Analysis Date = 08/02/14 Pct Recovery = 64% Analysis Date = 08/02/14 Pct Recovery = 64% Analysis Date = 07/28/14 Pct Recovery = 64% Analysis Date = 07/28/14 Pct Recovery = 64% Analysis Date = 07/23/14 Pct Recovery = 64% Analysis Date = 07/23/14 Pct Recovery = 64% Analysis Date = 07/18/14 Pct Recovery = 64% Analysis Date = 07/18/14 Pct Recovery = 64% Analysis Date = 07/13/14 Pct Recovery = 64% Analysis Date = 07/13/14 Pct Recovery = 64% Analysis Date = 07/08/14 Pct Recovery = 64% Analysis Date = 07/08/14 Pct Recovery = 64% Analysis Date = 07/03/14 Pct Recovery = 64% Analysis Date = 07/03/14 Pct Recovery = 64% Analysis Date = 06/28/14 Pct Recovery = 64% Analysis Date = 06/28/14 Pct Recovery = 64% Analysis Date = 06/24/14 Pct Recovery = 64% Analysis Date = 06/24/14 Pct Recovery = 64% Analysis Date = 06/19/14 Pct Recovery = 63% Analysis Date = 06/19/14 Pct Recovery = 63% Analysis Date = 06/14/14 Pct Recovery = 63% Analysis Date = 06/14/14 Pct Recovery = 63% Analysis Date = 06/09/14 Pct Recovery = 63% Analysis Date = 06/09/14 Pct Recovery = 63% Analysis Date = 06/04/14 Pct Recovery = 63% Analysis Date = 06/04/14 Pct Recovery = 63% Analysis Date = 05/30/14 Pct Recovery = 63% Analysis Date = 05/30/14 Pct Recovery = 63% Analysis Date = 05/25/14 Pct Recovery = 63% Analysis Date = 05/25/14 Pct Recovery = 63% Analysis Date = 05/21/14 Pct Recovery = 63% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
VENLAFAXINE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 1 64% . 64% 0%
>= Reporting Level 68 64% 13% 63% 14%
Total 69 64% 13% 63% 14%

Sample Statistics
VENLAFAXINE

Characteristic N % % Basis
Plotted 69 92% Spiked
Estimated Values 4 5% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 1 1% Spiked
Spiked 75 .  
False Negatives 5 7% 5 out of 75
Not Spiked 40 .  
False Positives 0 0% 0 out of 40

BQS OBSP Determination:
VERAPAMIL
METHOD: 2440 , TESTIDCODE: 67472LCM56
Open Data Set

Analysis Date = 01/17/16 SpikeMix = ERA 0406-15-09: 80 µl & ERA 0406-15-07A: 80 µl Pct Recovery = 43% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 80 µl & Abs 051315: 80 µl Pct Recovery = 29% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 80 µl & ERA 0406-15-08: 80 µl Pct Recovery = 24% Analysis Date = 11/04/15 SpikeMix = Abs 052215: 80 µl & Abs 050115: 80 µl Pct Recovery = 39% Analysis Date = 09/24/16 SpikeMix = Crescent EN160610015: 80 µl & Abs 061416: 80 µl Pct Recovery = 24% Analysis Date = 09/24/16 SpikeMix = Abs 061416: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 24% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 29% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 44% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 59% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 68% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-04: 15 µl & Abs 041814: 15 µl Pct Recovery = 20% Analysis Date = 12/06/14 SpikeMix = ERA 0318-14-02: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 21% Analysis Date = 10/25/14 SpikeMix = Abs 041614: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 19% Analysis Date = 10/11/14 SpikeMix = ERA 0318-14-02: 60 µl & ERA 0319-14-04: 60 µl Pct Recovery = 34% Analysis Date = 08/28/14 SpikeMix = ERA 0319-14-04: 60 µl & ERA 0319-14-05: 60 µl Pct Recovery = 23% Analysis Date = 05/07/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 25% Analysis Date = 03/11/15 SpikeMix = ERA 0318-14-02: 15 µl & Abs 041714: 15 µl Pct Recovery = 38% Analysis Date = 01/16/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 30% Analysis Date = 12/06/14 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 26% Analysis Date = 08/21/14 SpikeMix = ERA 0318-14-02: 60 µl & Abs 041714: 60 µl Pct Recovery = 11% Analysis Date = 07/12/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 48% Analysis Date = 06/11/14 SpikeMix = Abs 041614: 60 µl & Abs 041714: 60 µl Pct Recovery = 26% Analysis Date = 05/21/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 46% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-07A: 40 µl & Abs 051315: 40 µl Pct Recovery = 42% Analysis Date = 11/04/15 SpikeMix = ERA 0406-15-07A: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 43% Analysis Date = 09/10/15 SpikeMix = Abs 052215: 40 µl & ERA 0406-15-07A: 40 µl Pct Recovery = 43% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 53% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 46% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 29% Analysis Date = 02/23/16 SpikeMix = Abs 052215: 40 µl & Abs 050115: 40 µl Pct Recovery = 51% Analysis Date = 07/31/15 SpikeMix = ERA 0406-15-09: 40 µl & Abs 050115: 40 µl Pct Recovery = 55% Analysis Date = 07/30/15 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 36% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 47% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 44% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 16% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 23% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 10% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 24% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 30% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 30% Analysis Date = 04/30/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 35% Analysis Date = 04/10/15 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 15% Analysis Date = 02/10/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 15% Analysis Date = 12/07/14 SpikeMix = ERA 0318-14-02: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 48% Analysis Date = 10/11/14 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 14% Analysis Date = 08/16/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 27% Analysis Date = 07/13/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 8% Analysis Date = 10/10/14 SpikeMix = Abs 041714: 30 µl & Abs 041814: 30 µl Pct Recovery = 26% Analysis Date = 06/28/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 15% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 72% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 70% Analysis Date = 04/27/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 56% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 41% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 23% Analysis Date = 11/24/15 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 31% Analysis Date = 09/15/15 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 51% Analysis Date = 11/25/15 SpikeMix = Abs 050115: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 31% Analysis Date = 11/24/15 SpikeMix = ERA 0406-15-09: 20 µl & Abs 050115: 20 µl Pct Recovery = 43% Analysis Date = 07/09/15 SpikeMix = Abs 050115: 20 µl & Abs 052215: 20 µl Pct Recovery = 29% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 49% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 43% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 24% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 36% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 29% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 24% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 25% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 23% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 112% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 116% Analysis Date = 01/18/17 Pct Recovery = 37% Analysis Date = 01/14/17 Pct Recovery = 38% Analysis Date = 01/14/17 Pct Recovery = 38% Analysis Date = 01/09/17 Pct Recovery = 38% Analysis Date = 01/09/17 Pct Recovery = 38% Analysis Date = 01/04/17 Pct Recovery = 38% Analysis Date = 01/04/17 Pct Recovery = 38% Analysis Date = 12/30/16 Pct Recovery = 38% Analysis Date = 12/30/16 Pct Recovery = 38% Analysis Date = 12/25/16 Pct Recovery = 38% Analysis Date = 12/25/16 Pct Recovery = 38% Analysis Date = 12/20/16 Pct Recovery = 38% Analysis Date = 12/20/16 Pct Recovery = 38% Analysis Date = 12/15/16 Pct Recovery = 38% Analysis Date = 12/15/16 Pct Recovery = 38% Analysis Date = 12/11/16 Pct Recovery = 39% Analysis Date = 12/11/16 Pct Recovery = 39% Analysis Date = 12/06/16 Pct Recovery = 39% Analysis Date = 12/06/16 Pct Recovery = 39% Analysis Date = 12/01/16 Pct Recovery = 39% Analysis Date = 12/01/16 Pct Recovery = 39% Analysis Date = 11/26/16 Pct Recovery = 39% Analysis Date = 11/26/16 Pct Recovery = 39% Analysis Date = 11/21/16 Pct Recovery = 39% Analysis Date = 11/21/16 Pct Recovery = 39% Analysis Date = 11/16/16 Pct Recovery = 39% Analysis Date = 11/16/16 Pct Recovery = 39% Analysis Date = 11/11/16 Pct Recovery = 39% Analysis Date = 11/11/16 Pct Recovery = 39% Analysis Date = 11/06/16 Pct Recovery = 40% Analysis Date = 11/06/16 Pct Recovery = 40% Analysis Date = 11/02/16 Pct Recovery = 40% Analysis Date = 11/02/16 Pct Recovery = 40% Analysis Date = 10/28/16 Pct Recovery = 40% Analysis Date = 10/28/16 Pct Recovery = 40% Analysis Date = 10/23/16 Pct Recovery = 40% Analysis Date = 10/23/16 Pct Recovery = 40% Analysis Date = 10/18/16 Pct Recovery = 40% Analysis Date = 10/18/16 Pct Recovery = 40% Analysis Date = 10/13/16 Pct Recovery = 40% Analysis Date = 10/13/16 Pct Recovery = 40% Analysis Date = 10/08/16 Pct Recovery = 41% Analysis Date = 10/08/16 Pct Recovery = 41% Analysis Date = 10/03/16 Pct Recovery = 41% Analysis Date = 10/03/16 Pct Recovery = 41% Analysis Date = 09/28/16 Pct Recovery = 41% Analysis Date = 09/28/16 Pct Recovery = 41% Analysis Date = 09/24/16 Pct Recovery = 41% Analysis Date = 09/24/16 Pct Recovery = 41% Analysis Date = 09/19/16 Pct Recovery = 41% Analysis Date = 09/19/16 Pct Recovery = 41% Analysis Date = 09/14/16 Pct Recovery = 41% Analysis Date = 09/14/16 Pct Recovery = 41% Analysis Date = 09/09/16 Pct Recovery = 42% Analysis Date = 09/09/16 Pct Recovery = 42% Analysis Date = 09/04/16 Pct Recovery = 42% Analysis Date = 09/04/16 Pct Recovery = 42% Analysis Date = 08/30/16 Pct Recovery = 42% Analysis Date = 08/30/16 Pct Recovery = 42% Analysis Date = 08/25/16 Pct Recovery = 42% Analysis Date = 08/25/16 Pct Recovery = 42% Analysis Date = 08/21/16 Pct Recovery = 42% Analysis Date = 08/21/16 Pct Recovery = 42% Analysis Date = 08/16/16 Pct Recovery = 42% Analysis Date = 08/16/16 Pct Recovery = 42% Analysis Date = 08/11/16 Pct Recovery = 42% Analysis Date = 08/11/16 Pct Recovery = 42% Analysis Date = 08/06/16 Pct Recovery = 42% Analysis Date = 08/06/16 Pct Recovery = 42% Analysis Date = 08/01/16 Pct Recovery = 42% Analysis Date = 08/01/16 Pct Recovery = 42% Analysis Date = 07/27/16 Pct Recovery = 42% Analysis Date = 07/27/16 Pct Recovery = 42% Analysis Date = 07/22/16 Pct Recovery = 42% Analysis Date = 07/22/16 Pct Recovery = 42% Analysis Date = 07/17/16 Pct Recovery = 42% Analysis Date = 07/17/16 Pct Recovery = 42% Analysis Date = 07/13/16 Pct Recovery = 42% Analysis Date = 07/13/16 Pct Recovery = 42% Analysis Date = 07/08/16 Pct Recovery = 42% Analysis Date = 07/08/16 Pct Recovery = 42% Analysis Date = 07/03/16 Pct Recovery = 42% Analysis Date = 07/03/16 Pct Recovery = 42% Analysis Date = 06/28/16 Pct Recovery = 42% Analysis Date = 06/28/16 Pct Recovery = 42% Analysis Date = 06/23/16 Pct Recovery = 42% Analysis Date = 06/23/16 Pct Recovery = 42% Analysis Date = 06/18/16 Pct Recovery = 42% Analysis Date = 06/18/16 Pct Recovery = 42% Analysis Date = 06/13/16 Pct Recovery = 42% Analysis Date = 06/13/16 Pct Recovery = 42% Analysis Date = 06/08/16 Pct Recovery = 42% Analysis Date = 06/08/16 Pct Recovery = 42% Analysis Date = 06/04/16 Pct Recovery = 42% Analysis Date = 06/04/16 Pct Recovery = 42% Analysis Date = 05/30/16 Pct Recovery = 42% Analysis Date = 05/30/16 Pct Recovery = 42% Analysis Date = 05/25/16 Pct Recovery = 42% Analysis Date = 05/25/16 Pct Recovery = 42% Analysis Date = 05/20/16 Pct Recovery = 42% Analysis Date = 05/20/16 Pct Recovery = 42% Analysis Date = 05/15/16 Pct Recovery = 42% Analysis Date = 05/15/16 Pct Recovery = 42% Analysis Date = 05/10/16 Pct Recovery = 42% Analysis Date = 05/10/16 Pct Recovery = 42% Analysis Date = 05/05/16 Pct Recovery = 42% Analysis Date = 05/05/16 Pct Recovery = 42% Analysis Date = 05/01/16 Pct Recovery = 42% Analysis Date = 05/01/16 Pct Recovery = 42% Analysis Date = 04/26/16 Pct Recovery = 42% Analysis Date = 04/26/16 Pct Recovery = 42% Analysis Date = 04/21/16 Pct Recovery = 42% Analysis Date = 04/21/16 Pct Recovery = 42% Analysis Date = 04/16/16 Pct Recovery = 42% Analysis Date = 04/16/16 Pct Recovery = 42% Analysis Date = 04/11/16 Pct Recovery = 42% Analysis Date = 04/11/16 Pct Recovery = 42% Analysis Date = 04/06/16 Pct Recovery = 42% Analysis Date = 04/06/16 Pct Recovery = 42% Analysis Date = 04/01/16 Pct Recovery = 42% Analysis Date = 04/01/16 Pct Recovery = 42% Analysis Date = 03/27/16 Pct Recovery = 42% Analysis Date = 03/27/16 Pct Recovery = 42% Analysis Date = 03/23/16 Pct Recovery = 42% Analysis Date = 03/23/16 Pct Recovery = 42% Analysis Date = 03/18/16 Pct Recovery = 42% Analysis Date = 03/18/16 Pct Recovery = 42% Analysis Date = 03/13/16 Pct Recovery = 42% Analysis Date = 03/13/16 Pct Recovery = 42% Analysis Date = 03/08/16 Pct Recovery = 42% Analysis Date = 03/08/16 Pct Recovery = 42% Analysis Date = 03/03/16 Pct Recovery = 42% Analysis Date = 03/03/16 Pct Recovery = 42% Analysis Date = 02/27/16 Pct Recovery = 42% Analysis Date = 02/27/16 Pct Recovery = 42% Analysis Date = 02/22/16 Pct Recovery = 42% Analysis Date = 02/22/16 Pct Recovery = 42% Analysis Date = 02/17/16 Pct Recovery = 42% Analysis Date = 02/17/16 Pct Recovery = 42% Analysis Date = 02/13/16 Pct Recovery = 42% Analysis Date = 02/13/16 Pct Recovery = 42% Analysis Date = 02/08/16 Pct Recovery = 42% Analysis Date = 02/08/16 Pct Recovery = 42% Analysis Date = 02/03/16 Pct Recovery = 42% Analysis Date = 02/03/16 Pct Recovery = 42% Analysis Date = 01/29/16 Pct Recovery = 42% Analysis Date = 01/29/16 Pct Recovery = 42% Analysis Date = 01/24/16 Pct Recovery = 42% Analysis Date = 01/24/16 Pct Recovery = 42% Analysis Date = 01/19/16 Pct Recovery = 42% Analysis Date = 01/19/16 Pct Recovery = 42% Analysis Date = 01/14/16 Pct Recovery = 42% Analysis Date = 01/14/16 Pct Recovery = 42% Analysis Date = 01/10/16 Pct Recovery = 41% Analysis Date = 01/10/16 Pct Recovery = 41% Analysis Date = 01/05/16 Pct Recovery = 41% Analysis Date = 01/05/16 Pct Recovery = 41% Analysis Date = 12/31/15 Pct Recovery = 41% Analysis Date = 12/31/15 Pct Recovery = 41% Analysis Date = 12/26/15 Pct Recovery = 41% Analysis Date = 12/26/15 Pct Recovery = 41% Analysis Date = 12/21/15 Pct Recovery = 41% Analysis Date = 12/21/15 Pct Recovery = 41% Analysis Date = 12/16/15 Pct Recovery = 40% Analysis Date = 12/16/15 Pct Recovery = 40% Analysis Date = 12/11/15 Pct Recovery = 40% Analysis Date = 12/11/15 Pct Recovery = 40% Analysis Date = 12/06/15 Pct Recovery = 40% Analysis Date = 12/06/15 Pct Recovery = 40% Analysis Date = 12/02/15 Pct Recovery = 40% Analysis Date = 12/02/15 Pct Recovery = 40% Analysis Date = 11/27/15 Pct Recovery = 40% Analysis Date = 11/27/15 Pct Recovery = 40% Analysis Date = 11/22/15 Pct Recovery = 39% Analysis Date = 11/22/15 Pct Recovery = 39% Analysis Date = 11/17/15 Pct Recovery = 39% Analysis Date = 11/17/15 Pct Recovery = 39% Analysis Date = 11/12/15 Pct Recovery = 39% Analysis Date = 11/12/15 Pct Recovery = 39% Analysis Date = 11/07/15 Pct Recovery = 39% Analysis Date = 11/07/15 Pct Recovery = 39% Analysis Date = 11/02/15 Pct Recovery = 39% Analysis Date = 11/02/15 Pct Recovery = 39% Analysis Date = 10/28/15 Pct Recovery = 38% Analysis Date = 10/28/15 Pct Recovery = 38% Analysis Date = 10/24/15 Pct Recovery = 38% Analysis Date = 10/24/15 Pct Recovery = 38% Analysis Date = 10/19/15 Pct Recovery = 38% Analysis Date = 10/19/15 Pct Recovery = 38% Analysis Date = 10/14/15 Pct Recovery = 38% Analysis Date = 10/14/15 Pct Recovery = 38% Analysis Date = 10/09/15 Pct Recovery = 38% Analysis Date = 10/09/15 Pct Recovery = 38% Analysis Date = 10/04/15 Pct Recovery = 37% Analysis Date = 10/04/15 Pct Recovery = 37% Analysis Date = 09/29/15 Pct Recovery = 37% Analysis Date = 09/29/15 Pct Recovery = 37% Analysis Date = 09/24/15 Pct Recovery = 37% Analysis Date = 09/24/15 Pct Recovery = 37% Analysis Date = 09/19/15 Pct Recovery = 37% Analysis Date = 09/19/15 Pct Recovery = 37% Analysis Date = 09/15/15 Pct Recovery = 37% Analysis Date = 09/15/15 Pct Recovery = 37% Analysis Date = 09/10/15 Pct Recovery = 36% Analysis Date = 09/10/15 Pct Recovery = 36% Analysis Date = 09/05/15 Pct Recovery = 36% Analysis Date = 09/05/15 Pct Recovery = 36% Analysis Date = 08/31/15 Pct Recovery = 36% Analysis Date = 08/31/15 Pct Recovery = 36% Analysis Date = 08/26/15 Pct Recovery = 36% Analysis Date = 08/26/15 Pct Recovery = 36% Analysis Date = 08/21/15 Pct Recovery = 36% Analysis Date = 08/21/15 Pct Recovery = 36% Analysis Date = 08/16/15 Pct Recovery = 35% Analysis Date = 08/16/15 Pct Recovery = 35% Analysis Date = 08/12/15 Pct Recovery = 35% Analysis Date = 08/12/15 Pct Recovery = 35% Analysis Date = 08/07/15 Pct Recovery = 35% Analysis Date = 08/07/15 Pct Recovery = 35% Analysis Date = 08/02/15 Pct Recovery = 35% Analysis Date = 08/02/15 Pct Recovery = 35% Analysis Date = 07/28/15 Pct Recovery = 35% Analysis Date = 07/28/15 Pct Recovery = 35% Analysis Date = 07/23/15 Pct Recovery = 34% Analysis Date = 07/23/15 Pct Recovery = 34% Analysis Date = 07/18/15 Pct Recovery = 34% Analysis Date = 07/18/15 Pct Recovery = 34% Analysis Date = 07/13/15 Pct Recovery = 34% Analysis Date = 07/13/15 Pct Recovery = 34% Analysis Date = 07/08/15 Pct Recovery = 34% Analysis Date = 07/08/15 Pct Recovery = 34% Analysis Date = 07/04/15 Pct Recovery = 34% Analysis Date = 07/04/15 Pct Recovery = 34% Analysis Date = 06/29/15 Pct Recovery = 34% Analysis Date = 06/29/15 Pct Recovery = 34% Analysis Date = 06/24/15 Pct Recovery = 33% Analysis Date = 06/24/15 Pct Recovery = 33% Analysis Date = 06/19/15 Pct Recovery = 33% Analysis Date = 06/19/15 Pct Recovery = 33% Analysis Date = 06/14/15 Pct Recovery = 33% Analysis Date = 06/14/15 Pct Recovery = 33% Analysis Date = 06/09/15 Pct Recovery = 33% Analysis Date = 06/09/15 Pct Recovery = 33% Analysis Date = 06/04/15 Pct Recovery = 33% Analysis Date = 06/04/15 Pct Recovery = 33% Analysis Date = 05/30/15 Pct Recovery = 33% Analysis Date = 05/30/15 Pct Recovery = 33% Analysis Date = 05/26/15 Pct Recovery = 33% Analysis Date = 05/26/15 Pct Recovery = 33% Analysis Date = 05/21/15 Pct Recovery = 32% Analysis Date = 05/21/15 Pct Recovery = 32% Analysis Date = 05/16/15 Pct Recovery = 32% Analysis Date = 05/16/15 Pct Recovery = 32% Analysis Date = 05/11/15 Pct Recovery = 32% Analysis Date = 05/11/15 Pct Recovery = 32% Analysis Date = 05/06/15 Pct Recovery = 32% Analysis Date = 05/06/15 Pct Recovery = 32% Analysis Date = 05/01/15 Pct Recovery = 32% Analysis Date = 05/01/15 Pct Recovery = 32% Analysis Date = 04/26/15 Pct Recovery = 32% Analysis Date = 04/26/15 Pct Recovery = 32% Analysis Date = 04/22/15 Pct Recovery = 31% Analysis Date = 04/22/15 Pct Recovery = 31% Analysis Date = 04/17/15 Pct Recovery = 31% Analysis Date = 04/17/15 Pct Recovery = 31% Analysis Date = 04/12/15 Pct Recovery = 31% Analysis Date = 04/12/15 Pct Recovery = 31% Analysis Date = 04/07/15 Pct Recovery = 31% Analysis Date = 04/07/15 Pct Recovery = 31% Analysis Date = 04/02/15 Pct Recovery = 31% Analysis Date = 04/02/15 Pct Recovery = 31% Analysis Date = 03/28/15 Pct Recovery = 31% Analysis Date = 03/28/15 Pct Recovery = 31% Analysis Date = 03/23/15 Pct Recovery = 31% Analysis Date = 03/23/15 Pct Recovery = 31% Analysis Date = 03/18/15 Pct Recovery = 30% Analysis Date = 03/18/15 Pct Recovery = 30% Analysis Date = 03/14/15 Pct Recovery = 30% Analysis Date = 03/14/15 Pct Recovery = 30% Analysis Date = 03/09/15 Pct Recovery = 30% Analysis Date = 03/09/15 Pct Recovery = 30% Analysis Date = 03/04/15 Pct Recovery = 30% Analysis Date = 03/04/15 Pct Recovery = 30% Analysis Date = 02/27/15 Pct Recovery = 30% Analysis Date = 02/27/15 Pct Recovery = 30% Analysis Date = 02/22/15 Pct Recovery = 30% Analysis Date = 02/22/15 Pct Recovery = 30% Analysis Date = 02/17/15 Pct Recovery = 30% Analysis Date = 02/17/15 Pct Recovery = 30% Analysis Date = 02/12/15 Pct Recovery = 29% Analysis Date = 02/12/15 Pct Recovery = 29% Analysis Date = 02/07/15 Pct Recovery = 29% Analysis Date = 02/07/15 Pct Recovery = 29% Analysis Date = 02/03/15 Pct Recovery = 29% Analysis Date = 02/03/15 Pct Recovery = 29% Analysis Date = 01/29/15 Pct Recovery = 29% Analysis Date = 01/29/15 Pct Recovery = 29% Analysis Date = 01/24/15 Pct Recovery = 29% Analysis Date = 01/24/15 Pct Recovery = 29% Analysis Date = 01/19/15 Pct Recovery = 29% Analysis Date = 01/19/15 Pct Recovery = 29% Analysis Date = 01/14/15 Pct Recovery = 29% Analysis Date = 01/14/15 Pct Recovery = 29% Analysis Date = 01/09/15 Pct Recovery = 29% Analysis Date = 01/09/15 Pct Recovery = 29% Analysis Date = 01/04/15 Pct Recovery = 28% Analysis Date = 01/04/15 Pct Recovery = 28% Analysis Date = 12/31/14 Pct Recovery = 28% Analysis Date = 12/31/14 Pct Recovery = 28% Analysis Date = 12/26/14 Pct Recovery = 28% Analysis Date = 12/26/14 Pct Recovery = 28% Analysis Date = 12/21/14 Pct Recovery = 28% Analysis Date = 12/21/14 Pct Recovery = 28% Analysis Date = 12/16/14 Pct Recovery = 28% Analysis Date = 12/16/14 Pct Recovery = 28% Analysis Date = 12/11/14 Pct Recovery = 28% Analysis Date = 12/11/14 Pct Recovery = 28% Analysis Date = 12/06/14 Pct Recovery = 28% Analysis Date = 12/06/14 Pct Recovery = 28% Analysis Date = 12/01/14 Pct Recovery = 28% Analysis Date = 12/01/14 Pct Recovery = 28% Analysis Date = 11/26/14 Pct Recovery = 27% Analysis Date = 11/26/14 Pct Recovery = 27% Analysis Date = 11/22/14 Pct Recovery = 27% Analysis Date = 11/22/14 Pct Recovery = 27% Analysis Date = 11/17/14 Pct Recovery = 27% Analysis Date = 11/17/14 Pct Recovery = 27% Analysis Date = 11/12/14 Pct Recovery = 27% Analysis Date = 11/12/14 Pct Recovery = 27% Analysis Date = 11/07/14 Pct Recovery = 27% Analysis Date = 11/07/14 Pct Recovery = 27% Analysis Date = 11/02/14 Pct Recovery = 27% Analysis Date = 11/02/14 Pct Recovery = 27% Analysis Date = 10/28/14 Pct Recovery = 27% Analysis Date = 10/28/14 Pct Recovery = 27% Analysis Date = 10/23/14 Pct Recovery = 27% Analysis Date = 10/23/14 Pct Recovery = 27% Analysis Date = 10/18/14 Pct Recovery = 27% Analysis Date = 10/18/14 Pct Recovery = 27% Analysis Date = 10/14/14 Pct Recovery = 26% Analysis Date = 10/14/14 Pct Recovery = 26% Analysis Date = 10/09/14 Pct Recovery = 26% Analysis Date = 10/09/14 Pct Recovery = 26% Analysis Date = 10/04/14 Pct Recovery = 26% Analysis Date = 10/04/14 Pct Recovery = 26% Analysis Date = 09/29/14 Pct Recovery = 26% Analysis Date = 09/29/14 Pct Recovery = 26% Analysis Date = 09/24/14 Pct Recovery = 26% Analysis Date = 09/24/14 Pct Recovery = 26% Analysis Date = 09/19/14 Pct Recovery = 26% Analysis Date = 09/19/14 Pct Recovery = 26% Analysis Date = 09/14/14 Pct Recovery = 26% Analysis Date = 09/14/14 Pct Recovery = 26% Analysis Date = 09/10/14 Pct Recovery = 26% Analysis Date = 09/10/14 Pct Recovery = 26% Analysis Date = 09/05/14 Pct Recovery = 25% Analysis Date = 09/05/14 Pct Recovery = 25% Analysis Date = 08/31/14 Pct Recovery = 25% Analysis Date = 08/31/14 Pct Recovery = 25% Analysis Date = 08/26/14 Pct Recovery = 25% Analysis Date = 08/26/14 Pct Recovery = 25% Analysis Date = 08/21/14 Pct Recovery = 25% Analysis Date = 08/21/14 Pct Recovery = 25% Analysis Date = 08/16/14 Pct Recovery = 25% Analysis Date = 08/16/14 Pct Recovery = 25% Analysis Date = 08/11/14 Pct Recovery = 25% Analysis Date = 08/11/14 Pct Recovery = 25% Analysis Date = 08/06/14 Pct Recovery = 25% Analysis Date = 08/06/14 Pct Recovery = 25% Analysis Date = 08/02/14 Pct Recovery = 25% Analysis Date = 08/02/14 Pct Recovery = 25% Analysis Date = 07/28/14 Pct Recovery = 25% Analysis Date = 07/28/14 Pct Recovery = 25% Analysis Date = 07/23/14 Pct Recovery = 24% Analysis Date = 07/23/14 Pct Recovery = 24% Analysis Date = 07/18/14 Pct Recovery = 24% Analysis Date = 07/18/14 Pct Recovery = 24% Analysis Date = 07/13/14 Pct Recovery = 24% Analysis Date = 07/13/14 Pct Recovery = 24% Analysis Date = 07/08/14 Pct Recovery = 24% Analysis Date = 07/08/14 Pct Recovery = 24% Analysis Date = 07/03/14 Pct Recovery = 24% Analysis Date = 07/03/14 Pct Recovery = 24% Analysis Date = 06/28/14 Pct Recovery = 24% Analysis Date = 06/28/14 Pct Recovery = 24% Analysis Date = 06/24/14 Pct Recovery = 24% Analysis Date = 06/24/14 Pct Recovery = 24% Analysis Date = 06/19/14 Pct Recovery = 24% Analysis Date = 06/19/14 Pct Recovery = 24% Analysis Date = 06/14/14 Pct Recovery = 24% Analysis Date = 06/14/14 Pct Recovery = 24% Analysis Date = 06/09/14 Pct Recovery = 24% Analysis Date = 06/09/14 Pct Recovery = 24% Analysis Date = 06/04/14 Pct Recovery = 23% Analysis Date = 06/04/14 Pct Recovery = 23% Analysis Date = 05/30/14 Pct Recovery = 23% Analysis Date = 05/30/14 Pct Recovery = 23% Analysis Date = 05/25/14 Pct Recovery = 23% Analysis Date = 05/25/14 Pct Recovery = 23% Analysis Date = 05/21/14 Pct Recovery = 23% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
VERAPAMIL

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 10 48% 36% 32% 18%
>= Reporting Level 59 34% 15% 30% 15%
Total 69 36% 20% 30% 15%

Sample Statistics
VERAPAMIL

Characteristic N % % Basis
Plotted 69 88% Spiked
Estimated Values 21 27% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 78 .  
False Negatives 9 12% 9 out of 78
Not Spiked 37 .  
False Positives 0 0% 0 out of 37

BQS OBSP Determination:
WARFARIN
METHOD: 2440 , TESTIDCODE: 67457LCM56
Open Data Set

Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 55% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 67% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 80 µl & ERA 0406-15-08: 80 µl Pct Recovery = 79% Analysis Date = 11/05/15 SpikeMix = ERA 0406-15-08: 80 µl & Abs 052215: 80 µl Pct Recovery = 73% Analysis Date = 11/24/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 71% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 80 µl & Abs 051315: 80 µl Pct Recovery = 77% Analysis Date = 10/01/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 105% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 63% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 63% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 84% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 78% Analysis Date = 11/18/16 SpikeMix = ERA 04281604: 80 µl & ERA 04281603: 80 µl Pct Recovery = 57% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & ERA 04281604: 80 µl Pct Recovery = 55% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 56% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 54% Analysis Date = 05/07/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 51% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 31% Analysis Date = 01/16/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 48% Analysis Date = 12/07/14 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 39% Analysis Date = 12/06/14 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 37% Analysis Date = 08/28/14 SpikeMix = ERA 0319-14-04: 60 µl & ERA 0319-14-05: 60 µl Pct Recovery = 35% Analysis Date = 07/26/14 SpikeMix = ERA 0319-14-05: 60 µl & ERA 0318-14-02: 60 µl Pct Recovery = 57% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-04: 15 µl & Abs 041814: 15 µl Pct Recovery = 64% Analysis Date = 02/06/15 SpikeMix = Abs 041814: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 68% Analysis Date = 07/12/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 71% Analysis Date = 06/22/14 SpikeMix = Abs 041814: 60 µl & Abs 041614: 60 µl Pct Recovery = 105% Analysis Date = 05/21/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 78% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-08: 40 µl & Abs 052215: 40 µl Pct Recovery = 70% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 68% Analysis Date = 11/04/15 SpikeMix = ERA 0406-15-07A: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 75% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-08: 40 µl & ERA 0406-15-09: 40 µl Pct Recovery = 48% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 88% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 76% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-07A: 40 µl & Abs 051315: 40 µl Pct Recovery = 76% Analysis Date = 07/31/15 SpikeMix = Abs 051315: 40 µl & Abs 052215: 40 µl Pct Recovery = 66% Analysis Date = 07/30/15 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 71% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 99% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 115% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 82% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 75% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 77% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 77% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 56% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 65% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 42% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 42% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 56% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 64% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 53% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 52% Analysis Date = 11/04/14 SpikeMix = Abs 041714: 8 µl & ERA 0319-14-05: 8 µl Pct Recovery = 33% Analysis Date = 10/24/14 SpikeMix = ERA 0319-14-05: 8 µl & Abs 041614: 8 µl Pct Recovery = 54% Analysis Date = 04/10/15 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 63% Analysis Date = 11/04/14 SpikeMix = Abs 041814: 8 µl & ERA 0318-14-02: 8 µl Pct Recovery = 54% Analysis Date = 10/11/14 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 42% Analysis Date = 08/30/14 SpikeMix = ERA 0318-14-02: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 50% Analysis Date = 08/16/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 29% Analysis Date = 07/13/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 42% Analysis Date = 10/10/14 SpikeMix = Abs 041714: 30 µl & Abs 041814: 30 µl Pct Recovery = 56% Analysis Date = 10/10/14 SpikeMix = Abs 041814: 30 µl & ERA 0318-14-02: 30 µl Pct Recovery = 47% Analysis Date = 07/13/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 57% Analysis Date = 05/30/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 69% Analysis Date = 04/27/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 111% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 94% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-08: 20 µl & ERA 0406-15-09: 20 µl Pct Recovery = 67% Analysis Date = 11/25/15 SpikeMix = Abs 050115: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 72% Analysis Date = 09/15/15 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 80% Analysis Date = 02/23/16 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 94% Analysis Date = 08/11/15 SpikeMix = Abs 050115: 20 µl & Abs 051315: 20 µl Pct Recovery = 56% Analysis Date = 06/26/15 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 67% Analysis Date = 06/09/15 SpikeMix = Abs 051315: 20 µl & Abs 050115: 20 µl Pct Recovery = 39% Analysis Date = 01/18/17 Pct Recovery = 65% Analysis Date = 01/14/17 Pct Recovery = 66% Analysis Date = 01/14/17 Pct Recovery = 66% Analysis Date = 01/09/17 Pct Recovery = 66% Analysis Date = 01/09/17 Pct Recovery = 66% Analysis Date = 01/04/17 Pct Recovery = 66% Analysis Date = 01/04/17 Pct Recovery = 66% Analysis Date = 12/30/16 Pct Recovery = 66% Analysis Date = 12/30/16 Pct Recovery = 66% Analysis Date = 12/25/16 Pct Recovery = 66% Analysis Date = 12/25/16 Pct Recovery = 66% Analysis Date = 12/20/16 Pct Recovery = 66% Analysis Date = 12/20/16 Pct Recovery = 66% Analysis Date = 12/15/16 Pct Recovery = 66% Analysis Date = 12/15/16 Pct Recovery = 66% Analysis Date = 12/11/16 Pct Recovery = 67% Analysis Date = 12/11/16 Pct Recovery = 67% Analysis Date = 12/06/16 Pct Recovery = 67% Analysis Date = 12/06/16 Pct Recovery = 67% Analysis Date = 12/01/16 Pct Recovery = 67% Analysis Date = 12/01/16 Pct Recovery = 67% Analysis Date = 11/26/16 Pct Recovery = 67% Analysis Date = 11/26/16 Pct Recovery = 67% Analysis Date = 11/21/16 Pct Recovery = 67% Analysis Date = 11/21/16 Pct Recovery = 67% Analysis Date = 11/16/16 Pct Recovery = 67% Analysis Date = 11/16/16 Pct Recovery = 67% Analysis Date = 11/11/16 Pct Recovery = 67% Analysis Date = 11/11/16 Pct Recovery = 67% Analysis Date = 11/06/16 Pct Recovery = 67% Analysis Date = 11/06/16 Pct Recovery = 67% Analysis Date = 11/02/16 Pct Recovery = 68% Analysis Date = 11/02/16 Pct Recovery = 68% Analysis Date = 10/28/16 Pct Recovery = 68% Analysis Date = 10/28/16 Pct Recovery = 68% Analysis Date = 10/23/16 Pct Recovery = 68% Analysis Date = 10/23/16 Pct Recovery = 68% Analysis Date = 10/18/16 Pct Recovery = 68% Analysis Date = 10/18/16 Pct Recovery = 68% Analysis Date = 10/13/16 Pct Recovery = 68% Analysis Date = 10/13/16 Pct Recovery = 68% Analysis Date = 10/08/16 Pct Recovery = 68% Analysis Date = 10/08/16 Pct Recovery = 68% Analysis Date = 10/03/16 Pct Recovery = 69% Analysis Date = 10/03/16 Pct Recovery = 69% Analysis Date = 09/28/16 Pct Recovery = 69% Analysis Date = 09/28/16 Pct Recovery = 69% Analysis Date = 09/24/16 Pct Recovery = 69% Analysis Date = 09/24/16 Pct Recovery = 69% Analysis Date = 09/19/16 Pct Recovery = 69% Analysis Date = 09/19/16 Pct Recovery = 69% Analysis Date = 09/14/16 Pct Recovery = 69% Analysis Date = 09/14/16 Pct Recovery = 69% Analysis Date = 09/09/16 Pct Recovery = 69% Analysis Date = 09/09/16 Pct Recovery = 69% Analysis Date = 09/04/16 Pct Recovery = 70% Analysis Date = 09/04/16 Pct Recovery = 70% Analysis Date = 08/30/16 Pct Recovery = 70% Analysis Date = 08/30/16 Pct Recovery = 70% Analysis Date = 08/25/16 Pct Recovery = 70% Analysis Date = 08/25/16 Pct Recovery = 70% Analysis Date = 08/21/16 Pct Recovery = 70% Analysis Date = 08/21/16 Pct Recovery = 70% Analysis Date = 08/16/16 Pct Recovery = 70% Analysis Date = 08/16/16 Pct Recovery = 70% Analysis Date = 08/11/16 Pct Recovery = 70% Analysis Date = 08/11/16 Pct Recovery = 70% Analysis Date = 08/06/16 Pct Recovery = 71% Analysis Date = 08/06/16 Pct Recovery = 71% Analysis Date = 08/01/16 Pct Recovery = 71% Analysis Date = 08/01/16 Pct Recovery = 71% Analysis Date = 07/27/16 Pct Recovery = 71% Analysis Date = 07/27/16 Pct Recovery = 71% Analysis Date = 07/22/16 Pct Recovery = 71% Analysis Date = 07/22/16 Pct Recovery = 71% Analysis Date = 07/17/16 Pct Recovery = 71% Analysis Date = 07/17/16 Pct Recovery = 71% Analysis Date = 07/13/16 Pct Recovery = 71% Analysis Date = 07/13/16 Pct Recovery = 71% Analysis Date = 07/08/16 Pct Recovery = 71% Analysis Date = 07/08/16 Pct Recovery = 71% Analysis Date = 07/03/16 Pct Recovery = 72% Analysis Date = 07/03/16 Pct Recovery = 72% Analysis Date = 06/28/16 Pct Recovery = 72% Analysis Date = 06/28/16 Pct Recovery = 72% Analysis Date = 06/23/16 Pct Recovery = 72% Analysis Date = 06/23/16 Pct Recovery = 72% Analysis Date = 06/18/16 Pct Recovery = 72% Analysis Date = 06/18/16 Pct Recovery = 72% Analysis Date = 06/13/16 Pct Recovery = 72% Analysis Date = 06/13/16 Pct Recovery = 72% Analysis Date = 06/08/16 Pct Recovery = 72% Analysis Date = 06/08/16 Pct Recovery = 72% Analysis Date = 06/04/16 Pct Recovery = 73% Analysis Date = 06/04/16 Pct Recovery = 73% Analysis Date = 05/30/16 Pct Recovery = 73% Analysis Date = 05/30/16 Pct Recovery = 73% Analysis Date = 05/25/16 Pct Recovery = 73% Analysis Date = 05/25/16 Pct Recovery = 73% Analysis Date = 05/20/16 Pct Recovery = 73% Analysis Date = 05/20/16 Pct Recovery = 73% Analysis Date = 05/15/16 Pct Recovery = 73% Analysis Date = 05/15/16 Pct Recovery = 73% Analysis Date = 05/10/16 Pct Recovery = 73% Analysis Date = 05/10/16 Pct Recovery = 73% Analysis Date = 05/05/16 Pct Recovery = 74% Analysis Date = 05/05/16 Pct Recovery = 74% Analysis Date = 05/01/16 Pct Recovery = 74% Analysis Date = 05/01/16 Pct Recovery = 74% Analysis Date = 04/26/16 Pct Recovery = 74% Analysis Date = 04/26/16 Pct Recovery = 74% Analysis Date = 04/21/16 Pct Recovery = 74% Analysis Date = 04/21/16 Pct Recovery = 74% Analysis Date = 04/16/16 Pct Recovery = 74% Analysis Date = 04/16/16 Pct Recovery = 74% Analysis Date = 04/11/16 Pct Recovery = 74% Analysis Date = 04/11/16 Pct Recovery = 74% Analysis Date = 04/06/16 Pct Recovery = 75% Analysis Date = 04/06/16 Pct Recovery = 75% Analysis Date = 04/01/16 Pct Recovery = 75% Analysis Date = 04/01/16 Pct Recovery = 75% Analysis Date = 03/27/16 Pct Recovery = 75% Analysis Date = 03/27/16 Pct Recovery = 75% Analysis Date = 03/23/16 Pct Recovery = 75% Analysis Date = 03/23/16 Pct Recovery = 75% Analysis Date = 03/18/16 Pct Recovery = 75% Analysis Date = 03/18/16 Pct Recovery = 75% Analysis Date = 03/13/16 Pct Recovery = 75% Analysis Date = 03/13/16 Pct Recovery = 75% Analysis Date = 03/08/16 Pct Recovery = 75% Analysis Date = 03/08/16 Pct Recovery = 75% Analysis Date = 03/03/16 Pct Recovery = 76% Analysis Date = 03/03/16 Pct Recovery = 76% Analysis Date = 02/27/16 Pct Recovery = 76% Analysis Date = 02/27/16 Pct Recovery = 76% Analysis Date = 02/22/16 Pct Recovery = 76% Analysis Date = 02/22/16 Pct Recovery = 76% Analysis Date = 02/17/16 Pct Recovery = 76% Analysis Date = 02/17/16 Pct Recovery = 76% Analysis Date = 02/13/16 Pct Recovery = 76% Analysis Date = 02/13/16 Pct Recovery = 76% Analysis Date = 02/08/16 Pct Recovery = 75% Analysis Date = 02/08/16 Pct Recovery = 75% Analysis Date = 02/03/16 Pct Recovery = 75% Analysis Date = 02/03/16 Pct Recovery = 75% Analysis Date = 01/29/16 Pct Recovery = 75% Analysis Date = 01/29/16 Pct Recovery = 75% Analysis Date = 01/24/16 Pct Recovery = 75% Analysis Date = 01/24/16 Pct Recovery = 75% Analysis Date = 01/19/16 Pct Recovery = 75% Analysis Date = 01/19/16 Pct Recovery = 75% Analysis Date = 01/14/16 Pct Recovery = 75% Analysis Date = 01/14/16 Pct Recovery = 75% Analysis Date = 01/10/16 Pct Recovery = 74% Analysis Date = 01/10/16 Pct Recovery = 74% Analysis Date = 01/05/16 Pct Recovery = 74% Analysis Date = 01/05/16 Pct Recovery = 74% Analysis Date = 12/31/15 Pct Recovery = 74% Analysis Date = 12/31/15 Pct Recovery = 74% Analysis Date = 12/26/15 Pct Recovery = 74% Analysis Date = 12/26/15 Pct Recovery = 74% Analysis Date = 12/21/15 Pct Recovery = 74% Analysis Date = 12/21/15 Pct Recovery = 74% Analysis Date = 12/16/15 Pct Recovery = 74% Analysis Date = 12/16/15 Pct Recovery = 74% Analysis Date = 12/11/15 Pct Recovery = 74% Analysis Date = 12/11/15 Pct Recovery = 74% Analysis Date = 12/06/15 Pct Recovery = 73% Analysis Date = 12/06/15 Pct Recovery = 73% Analysis Date = 12/02/15 Pct Recovery = 73% Analysis Date = 12/02/15 Pct Recovery = 73% Analysis Date = 11/27/15 Pct Recovery = 73% Analysis Date = 11/27/15 Pct Recovery = 73% Analysis Date = 11/22/15 Pct Recovery = 73% Analysis Date = 11/22/15 Pct Recovery = 73% Analysis Date = 11/17/15 Pct Recovery = 73% Analysis Date = 11/17/15 Pct Recovery = 73% Analysis Date = 11/12/15 Pct Recovery = 72% Analysis Date = 11/12/15 Pct Recovery = 72% Analysis Date = 11/07/15 Pct Recovery = 72% Analysis Date = 11/07/15 Pct Recovery = 72% Analysis Date = 11/02/15 Pct Recovery = 72% Analysis Date = 11/02/15 Pct Recovery = 72% Analysis Date = 10/28/15 Pct Recovery = 71% Analysis Date = 10/28/15 Pct Recovery = 71% Analysis Date = 10/24/15 Pct Recovery = 71% Analysis Date = 10/24/15 Pct Recovery = 71% Analysis Date = 10/19/15 Pct Recovery = 71% Analysis Date = 10/19/15 Pct Recovery = 71% Analysis Date = 10/14/15 Pct Recovery = 71% Analysis Date = 10/14/15 Pct Recovery = 71% Analysis Date = 10/09/15 Pct Recovery = 70% Analysis Date = 10/09/15 Pct Recovery = 70% Analysis Date = 10/04/15 Pct Recovery = 70% Analysis Date = 10/04/15 Pct Recovery = 70% Analysis Date = 09/29/15 Pct Recovery = 70% Analysis Date = 09/29/15 Pct Recovery = 70% Analysis Date = 09/24/15 Pct Recovery = 69% Analysis Date = 09/24/15 Pct Recovery = 69% Analysis Date = 09/19/15 Pct Recovery = 69% Analysis Date = 09/19/15 Pct Recovery = 69% Analysis Date = 09/15/15 Pct Recovery = 69% Analysis Date = 09/15/15 Pct Recovery = 69% Analysis Date = 09/10/15 Pct Recovery = 68% Analysis Date = 09/10/15 Pct Recovery = 68% Analysis Date = 09/05/15 Pct Recovery = 68% Analysis Date = 09/05/15 Pct Recovery = 68% Analysis Date = 08/31/15 Pct Recovery = 67% Analysis Date = 08/31/15 Pct Recovery = 67% Analysis Date = 08/26/15 Pct Recovery = 67% Analysis Date = 08/26/15 Pct Recovery = 67% Analysis Date = 08/21/15 Pct Recovery = 67% Analysis Date = 08/21/15 Pct Recovery = 67% Analysis Date = 08/16/15 Pct Recovery = 66% Analysis Date = 08/16/15 Pct Recovery = 66% Analysis Date = 08/12/15 Pct Recovery = 66% Analysis Date = 08/12/15 Pct Recovery = 66% Analysis Date = 08/07/15 Pct Recovery = 65% Analysis Date = 08/07/15 Pct Recovery = 65% Analysis Date = 08/02/15 Pct Recovery = 65% Analysis Date = 08/02/15 Pct Recovery = 65% Analysis Date = 07/28/15 Pct Recovery = 65% Analysis Date = 07/28/15 Pct Recovery = 65% Analysis Date = 07/23/15 Pct Recovery = 64% Analysis Date = 07/23/15 Pct Recovery = 64% Analysis Date = 07/18/15 Pct Recovery = 64% Analysis Date = 07/18/15 Pct Recovery = 64% Analysis Date = 07/13/15 Pct Recovery = 64% Analysis Date = 07/13/15 Pct Recovery = 64% Analysis Date = 07/08/15 Pct Recovery = 63% Analysis Date = 07/08/15 Pct Recovery = 63% Analysis Date = 07/04/15 Pct Recovery = 63% Analysis Date = 07/04/15 Pct Recovery = 63% Analysis Date = 06/29/15 Pct Recovery = 63% Analysis Date = 06/29/15 Pct Recovery = 63% Analysis Date = 06/24/15 Pct Recovery = 62% Analysis Date = 06/24/15 Pct Recovery = 62% Analysis Date = 06/19/15 Pct Recovery = 62% Analysis Date = 06/19/15 Pct Recovery = 62% Analysis Date = 06/14/15 Pct Recovery = 62% Analysis Date = 06/14/15 Pct Recovery = 62% Analysis Date = 06/09/15 Pct Recovery = 61% Analysis Date = 06/09/15 Pct Recovery = 61% Analysis Date = 06/04/15 Pct Recovery = 61% Analysis Date = 06/04/15 Pct Recovery = 61% Analysis Date = 05/30/15 Pct Recovery = 61% Analysis Date = 05/30/15 Pct Recovery = 61% Analysis Date = 05/26/15 Pct Recovery = 60% Analysis Date = 05/26/15 Pct Recovery = 60% Analysis Date = 05/21/15 Pct Recovery = 60% Analysis Date = 05/21/15 Pct Recovery = 60% Analysis Date = 05/16/15 Pct Recovery = 59% Analysis Date = 05/16/15 Pct Recovery = 59% Analysis Date = 05/11/15 Pct Recovery = 59% Analysis Date = 05/11/15 Pct Recovery = 59% Analysis Date = 05/06/15 Pct Recovery = 59% Analysis Date = 05/06/15 Pct Recovery = 59% Analysis Date = 05/01/15 Pct Recovery = 58% Analysis Date = 05/01/15 Pct Recovery = 58% Analysis Date = 04/26/15 Pct Recovery = 58% Analysis Date = 04/26/15 Pct Recovery = 58% Analysis Date = 04/22/15 Pct Recovery = 58% Analysis Date = 04/22/15 Pct Recovery = 58% Analysis Date = 04/17/15 Pct Recovery = 57% Analysis Date = 04/17/15 Pct Recovery = 57% Analysis Date = 04/12/15 Pct Recovery = 57% Analysis Date = 04/12/15 Pct Recovery = 57% Analysis Date = 04/07/15 Pct Recovery = 57% Analysis Date = 04/07/15 Pct Recovery = 57% Analysis Date = 04/02/15 Pct Recovery = 57% Analysis Date = 04/02/15 Pct Recovery = 57% Analysis Date = 03/28/15 Pct Recovery = 57% Analysis Date = 03/28/15 Pct Recovery = 57% Analysis Date = 03/23/15 Pct Recovery = 57% Analysis Date = 03/23/15 Pct Recovery = 57% Analysis Date = 03/18/15 Pct Recovery = 56% Analysis Date = 03/18/15 Pct Recovery = 56% Analysis Date = 03/14/15 Pct Recovery = 56% Analysis Date = 03/14/15 Pct Recovery = 56% Analysis Date = 03/09/15 Pct Recovery = 56% Analysis Date = 03/09/15 Pct Recovery = 56% Analysis Date = 03/04/15 Pct Recovery = 56% Analysis Date = 03/04/15 Pct Recovery = 56% Analysis Date = 02/27/15 Pct Recovery = 56% Analysis Date = 02/27/15 Pct Recovery = 56% Analysis Date = 02/22/15 Pct Recovery = 56% Analysis Date = 02/22/15 Pct Recovery = 56% Analysis Date = 02/17/15 Pct Recovery = 56% Analysis Date = 02/17/15 Pct Recovery = 56% Analysis Date = 02/12/15 Pct Recovery = 56% Analysis Date = 02/12/15 Pct Recovery = 56% Analysis Date = 02/07/15 Pct Recovery = 56% Analysis Date = 02/07/15 Pct Recovery = 56% Analysis Date = 02/03/15 Pct Recovery = 56% Analysis Date = 02/03/15 Pct Recovery = 56% Analysis Date = 01/29/15 Pct Recovery = 56% Analysis Date = 01/29/15 Pct Recovery = 56% Analysis Date = 01/24/15 Pct Recovery = 56% Analysis Date = 01/24/15 Pct Recovery = 56% Analysis Date = 01/19/15 Pct Recovery = 56% Analysis Date = 01/19/15 Pct Recovery = 56% Analysis Date = 01/14/15 Pct Recovery = 55% Analysis Date = 01/14/15 Pct Recovery = 55% Analysis Date = 01/09/15 Pct Recovery = 55% Analysis Date = 01/09/15 Pct Recovery = 55% Analysis Date = 01/04/15 Pct Recovery = 55% Analysis Date = 01/04/15 Pct Recovery = 55% Analysis Date = 12/31/14 Pct Recovery = 55% Analysis Date = 12/31/14 Pct Recovery = 55% Analysis Date = 12/26/14 Pct Recovery = 55% Analysis Date = 12/26/14 Pct Recovery = 55% Analysis Date = 12/21/14 Pct Recovery = 55% Analysis Date = 12/21/14 Pct Recovery = 55% Analysis Date = 12/16/14 Pct Recovery = 55% Analysis Date = 12/16/14 Pct Recovery = 55% Analysis Date = 12/11/14 Pct Recovery = 55% Analysis Date = 12/11/14 Pct Recovery = 55% Analysis Date = 12/06/14 Pct Recovery = 55% Analysis Date = 12/06/14 Pct Recovery = 55% Analysis Date = 12/01/14 Pct Recovery = 55% Analysis Date = 12/01/14 Pct Recovery = 55% Analysis Date = 11/26/14 Pct Recovery = 55% Analysis Date = 11/26/14 Pct Recovery = 55% Analysis Date = 11/22/14 Pct Recovery = 55% Analysis Date = 11/22/14 Pct Recovery = 55% Analysis Date = 11/17/14 Pct Recovery = 55% Analysis Date = 11/17/14 Pct Recovery = 55% Analysis Date = 11/12/14 Pct Recovery = 55% Analysis Date = 11/12/14 Pct Recovery = 55% Analysis Date = 11/07/14 Pct Recovery = 55% Analysis Date = 11/07/14 Pct Recovery = 55% Analysis Date = 11/02/14 Pct Recovery = 55% Analysis Date = 11/02/14 Pct Recovery = 55% Analysis Date = 10/28/14 Pct Recovery = 55% Analysis Date = 10/28/14 Pct Recovery = 55% Analysis Date = 10/23/14 Pct Recovery = 55% Analysis Date = 10/23/14 Pct Recovery = 55% Analysis Date = 10/18/14 Pct Recovery = 55% Analysis Date = 10/18/14 Pct Recovery = 55% Analysis Date = 10/14/14 Pct Recovery = 55% Analysis Date = 10/14/14 Pct Recovery = 55% Analysis Date = 10/09/14 Pct Recovery = 55% Analysis Date = 10/09/14 Pct Recovery = 55% Analysis Date = 10/04/14 Pct Recovery = 55% Analysis Date = 10/04/14 Pct Recovery = 55% Analysis Date = 09/29/14 Pct Recovery = 55% Analysis Date = 09/29/14 Pct Recovery = 55% Analysis Date = 09/24/14 Pct Recovery = 55% Analysis Date = 09/24/14 Pct Recovery = 55% Analysis Date = 09/19/14 Pct Recovery = 55% Analysis Date = 09/19/14 Pct Recovery = 55% Analysis Date = 09/14/14 Pct Recovery = 55% Analysis Date = 09/14/14 Pct Recovery = 55% Analysis Date = 09/10/14 Pct Recovery = 55% Analysis Date = 09/10/14 Pct Recovery = 55% Analysis Date = 09/05/14 Pct Recovery = 55% Analysis Date = 09/05/14 Pct Recovery = 55% Analysis Date = 08/31/14 Pct Recovery = 55% Analysis Date = 08/31/14 Pct Recovery = 55% Analysis Date = 08/26/14 Pct Recovery = 55% Analysis Date = 08/26/14 Pct Recovery = 55% Analysis Date = 08/21/14 Pct Recovery = 55% Analysis Date = 08/21/14 Pct Recovery = 55% Analysis Date = 08/16/14 Pct Recovery = 55% Analysis Date = 08/16/14 Pct Recovery = 55% Analysis Date = 08/11/14 Pct Recovery = 55% Analysis Date = 08/11/14 Pct Recovery = 55% Analysis Date = 08/06/14 Pct Recovery = 55% Analysis Date = 08/06/14 Pct Recovery = 55% Analysis Date = 08/02/14 Pct Recovery = 55% Analysis Date = 08/02/14 Pct Recovery = 55% Analysis Date = 07/28/14 Pct Recovery = 55% Analysis Date = 07/28/14 Pct Recovery = 55% Analysis Date = 07/23/14 Pct Recovery = 55% Analysis Date = 07/23/14 Pct Recovery = 55% Analysis Date = 07/18/14 Pct Recovery = 55% Analysis Date = 07/18/14 Pct Recovery = 55% Analysis Date = 07/13/14 Pct Recovery = 55% Analysis Date = 07/13/14 Pct Recovery = 55% Analysis Date = 07/08/14 Pct Recovery = 55% Analysis Date = 07/08/14 Pct Recovery = 55% Analysis Date = 07/03/14 Pct Recovery = 55% Analysis Date = 07/03/14 Pct Recovery = 55% Analysis Date = 06/28/14 Pct Recovery = 55% Analysis Date = 06/28/14 Pct Recovery = 55% Analysis Date = 06/24/14 Pct Recovery = 55% Analysis Date = 06/24/14 Pct Recovery = 55% Analysis Date = 06/19/14 Pct Recovery = 55% Analysis Date = 06/19/14 Pct Recovery = 55% Analysis Date = 06/14/14 Pct Recovery = 55% Analysis Date = 06/14/14 Pct Recovery = 55% Analysis Date = 06/09/14 Pct Recovery = 55% Analysis Date = 06/09/14 Pct Recovery = 55% Analysis Date = 06/04/14 Pct Recovery = 55% Analysis Date = 06/04/14 Pct Recovery = 55% Analysis Date = 05/30/14 Pct Recovery = 55% Analysis Date = 05/30/14 Pct Recovery = 55% Analysis Date = 05/25/14 Pct Recovery = 55% Analysis Date = 05/25/14 Pct Recovery = 55% Analysis Date = 05/21/14 Pct Recovery = 55% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
WARFARIN

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 71 65% 19% 64% 17%
Total 71 65% 19% 64% 17%

Sample Statistics
WARFARIN

Characteristic N % % Basis
Plotted 71 95% Spiked
Estimated Values 14 19% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 2 3% Spiked
Spiked 75 .  
False Negatives 2 3% 2 out of 75
Not Spiked 40 .  
False Positives 0 0% 0 out of 40